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HomeMy WebLinkAboutDRC-2022-022209 - 0901a0688110d17eOctober 21, 2022 Sent VIA OVERNIGHT DELIVERY Mr. Doug Hansen Director Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West Salt Lake City, UT 84116 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www.energyfuels.com Re: Transmittal of 3rd Quarter 2022 Groundwater Monitoring Report Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr. Hansen: Enclosed are two copies of the White Mesa Uranium Mill Groundwater Monitoring Report for the 3rd Quarter of 2022 as required by the Groundwater Quality Discharge Permit UGW370004, as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours very truly, «/(Mtj ½-� ENERGY FUELS RESOURCES {USA) INC. Kathy Weinel Director, Regulatory Compliance cc: David Frydenlund Scott Bakken Logan Shumway Garrin Palmer Jordan App DRC-2022-022209 INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports -Quarterly Sampling Tab F Laboratory Analytical Reports -Accelerated Monitoring Tab G Quality Assurance and Data Validation Tables G-lA/B G-2A/B G-3A/BG-4A/B G-5NBG-6A/B G-7A/B G-8A/BG-9AIB Field Data QNQC Evaluation Holding Time Evaluation Laboratory Receipt Temperature Check Analytical Method Check Reporting Limit Evaluation Trip Blank Evaluation QNQC Evaluation for Sample Duplicates Radiologies Counting En-or Laboratory Matrix QC Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter ii •The groundwater monitoring wells (including general monitoring wells, quarterlyand semi-annual monitoring wells, and (MW-34). •Existing monitoring well MW-4 and the temporary chloroform investigationwells. •Piezometers -P-1, P-2, P-3A, P-4 and P-5. •Nitrate monitoring wells. •The DR piezometers which were installed during the Southwest Hydrogeologic Investigation. •In addition to the above, depth to water measurements are routinely observed inconjunction with sampling events for wells sampled during quarterly and accelerated efforts, regardless of the sampling purpose. Water levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab D. 2.2 Field Data Attached under Tab B are copies of field data sheets recorded in association with the quarterly effort for the groundwater compliance monitoring wells referred to in paragraph 2.1.1, above. Sampling dates are listed in Table 1. Attached under Tab C, are copies of field data sheets recorded in association with the accelerated monthly monitoring sampling efforts, referred to in paragraph 2.1.2, above. Sampling dates are listed in Table 1. 2.3 Laboratory Results -Quarterly Sampling 2.3.1 Copy of Laboratory Results Analytical results are provided by two contract analytical laboratories: GEL and Chemtech-Ford ("CTF"). Table 1 lists the dates when analytical results were reported to the Director, Regulatory Compliance for each well. Results from analysis of samples collected under the GWDP (i.e., regular quarterly and accelerated semi-annual samples) are provided in Tab E. Also included under Tab E are the results of analyses for duplicate samples as identified in Table 1. 3 2.4.2 Regulatory Framework and Groundwater Background 2.4.3 Compliance Status 2.5 Depth to Groundwater and Water Table Contour Map There are three purging strategies specified in the QAP that are used to remove stagnant water from the casing during groundwater sampling at the Mill. The three strategies are as follows: 1.Purging three well casing volumes with a single measurement of field parameters2.Purging two casing volumes with stable field parameters (within 10% [RelativePercent Difference] ("RPD"))3.Purging a well to dryness and stability (within 10% RPD) of a limited list of fieldparameters after recovery During both the quarterly sampling event and the two monthly events, the purging technique used was two casing volumes with stable field parameters (pH, Conductivity, Redox, temperature, DO, and turbidity) except for the following wells that were purged to dryness: MW-24, MW-24A and MW-38. MW-24, MW-24A, and MW-38 conformed to the QAP requirement for sampling low yield wells which includes the collection of three field parameters (pH, specific conductance ["conductivity"] and temperature) immediately prior to and immediately following sample collection. Stabilization of pH, conductivity and temperature were within the 10% RPD required by the QAP. MW-24, MW-24A, and MW-38 were purged to dryness and the low yield sampling procedures were used for the collection of field parameters. Stabilization of pH, conductivity and temperature were within the 10% RPD required by the QAP for well MW-24, MW-24A, and MW-38. Additionally, two casing volumes were not purged from MW-26, prior to sampling because MW-26 is a continuously pumped well. If a well is continuously pumped, it is pumped on a set schedule per the remediation plan and is considered sufficiently evacuated to immediately collect a sample; however, if a pumping well has been out of service for 48 hours or more, EFRI follows the purging requirements outlined in Attachment 2-3 of the QAP. The review of the field sheets for compliance with QAP requirements resulted in the observations noted below. The QAP requirements in Attachment 2-3 specifically state that field parameters must be stabilized to within 10% over at least two consecutive measurements. The QAP Attachment 2-3 states that turbidity should be less than 5 NTU prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP Attachment 2-3 does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements greater than 5 NTU below are included for information purposes only. •Turbidity measurements were less than 5 NTU for the quarterly and semi-annualwells except MW-11, MW-29, and MW-32. Per the QAP, Attachment 2-3,turbidity measurements prior to sampling were within a 10% RPD for thequarterly and semi-annual wells. 8 •Turbidity measurements were less than 5 NTU for the accelerated sampling wellsexcept MW-11. Per the QAP, Attachment 2-3, turbidity measurements prior tosampling were within a 10% RPD for the quarterly and semi-annual wells.Turbidity measurements prior to sampling were within a 10% RPD for theaccelerated sampling wells.The other field parameters (conductance, pH, redox potential, DO, and temperature) for the wells were within the required RPD for the quarterly, semi-annual and accelerated sampling. During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water for the quarterly, semi-annual and accelerated sampling programs to the nearest 0.01 foot. EFRI's letter to DWMRC of March 26, 2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In response to DWMRC's subsequent correspondence dated June 1, 2010 and June 24, 2010, EFRI has completed a monitoring well redevelopment program. The redevelopment report was submitted to DWMRC on September 30, 2011. DWMRC responded to the redevelopment report via letter on November 15, 2012. Per the DWMRC letter dated November 15, 2012, the field data generated this quarter are compliant with the turbidity requirements of the approved QAP. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided under Tab G. The samples were received and analyzed within the required holding time. All accelerated samples were received and analyzed within the required holding time. 3.4.3 Receipt Temperature Evaluation COC sheets were reviewed to confirm compliance with the QAP requirement in Table 1 that samples be received at 6°C or lower. Sample receipt temperature checks are provided under Tab G. The quarterly, semi-annual and accelerated samples were received within the required temperature limit. As noted in Tab G, samples for gross alpha analyses were shipped without using ice. Per Table 1 in the approved QAP, samples submitted for gross alpha analyses do not have a sample temperature requirement. 3.4.4 Analytical Method Checklist The analytical methods reported by both laboratories were checked against the required methods specified in the QAP. Analytical method check results are provided in Tab G. 9 The review indicated that the quarterly, semi-annual and accelerated samples were analyzed in accordance with Table 1 of the QAP. 3.4.5 Reporting Limit Evaluation The analytical method RLs reported by both laboratories were checked against the RLs specified in the QAP Table 1. RL evaluations are provided in Tab G. The analytes were measured and reported to the required RLs except that several sets of quarterly, semi­annual and accelerated sample results had the RL raised for at least one analyte due to matrix interference and/or sample dilution as noted in Section 3.4.9. In all cases the reported value for the analyte was higher than the increased RL. 3.4.6 Trip Blank Evaluation The trip blank results were reviewed to identify any VOC sample contamination which is the result of sample handling and shipment. Trip blank evaluations are provided in Tab G.The trip blank results associated with the quarterly, semi-annual and acceleratedsamples were all nondetect for VOCs.3.4.7 QA/QC Evaluation for Routine Sample Duplicates Section 9 .1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results are less than 5 times the detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for the duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits; however, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPD is greater than 20%. The additional duplicate information is provided for information purposes. Field duplicate sample results were assessed as required by the QAP. Duplicate results were within the acceptance limits specified in the QAP except for fluoride in MW-38/MW-65. The fluoride results were not greater than 5 times the RL and as such are acceptable. Field duplicate results are shown in Attachment G. The duplicate results were within a 20% RPD in the accelerated samples. Results of the RPD test are provided under Tab G. 3.4.8 Radiologies Counting Error and Duplicate Evaluation Section 9 .14 of the QAP requires that when gross alpha results are reported with an activity equal to or greater than the GWCL the counting variance shall be equal to or less than 20% of the reported activity concentration. An error term may be greater than 20% 10 of the reported activity concentration when the sum of the activity concentration and error term is less than or equal to the GWCL. The quarterly and semi-annual radiologic sample results met the counting error requirements specified in the QAP except as noted in Tab G. The results for MW-26, MW-31, and MW-39 did not meet the requirement that the counting error be equal to or less than 20% of the reported activity concentration, likely because the reported concentrations are very near the RL. As stated above the error term may be greater than 20% of the reported activity concentration when the sum of the activity concentration and error term is less than or equal to the GWCL; however MW-39 does not have a GWCL and this second level check cannot be performed. MW-26 and MW-31 passed the secondary check. The results are usable for the intended purpose and there is no adverse effect on the data. Section 9.4 of the QAP also requires a comparability check between the sample and field duplicate sample results utilizing the formula provided in the text. Results of quarterly and semi-annual, radiologic sample QC are provided under Tab G. The quarterly and semi-annual sample results met the duplicate counting error requirements specified in the QAP. 3.4.9 Other Laboratory QA/QC Section 9.2 of the QAP requires that the laboratory's QA/QC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate analytical laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, EFRI's Director, Regulatory Compliance rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided under Tab G. The lab QA/QC results from both GEL and CTF samples for compounds regulated under the GWDP met these requirements. The check samples included at least the following: a method blank, a laboratory control spike ("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the equivalent, where applicable. It should be noted that: •Laboratory fortified blanks are equivalent to LCSs.•Laboratory reagent blanks are equivalent to method blanks.•Post digestion spikes are equivalent to MSs.•Post digestion spike duplicates are equivalent to MSDs.•Laboratory Duplicates are equivalent to MSDs.11 Monitoring Well(Water Constituent Exceeding GWCL Class) Nitrate+ Nit1ite (as N) (n,g/L) MW-II Chloride (mg/L) (Class II) Manganese (.ug/L) Sulfate (m�L) TDS (mg/L) MW-25 (Class TDS (mg/L) 111) Nitrate+ Nitrite (as Nl (ml:IL) MW-26 Chloroform (u�/l.) (Class Ill) Chloride (mg/L) TDS (ml!/L) Nitrate+ Nitrite (ns N) (111!1/t) MW-30 Chloride (mg/L) Selenium (ug/L) (Class II) TDS (mg/L) Uranium (ug/L) Nitrate+ Nitrite (ns N) (ml!/L) MW-31 Sulfate (mg/L) (Class 111) TDS (tnl!/L) Uranium (ug/L) Chloride (111g/L) MW-12 Uranium (u!!/L) (Class lll) Selenium (ug/L) Beryllium (ul!/L) Cadmium (uJl/L) Fluoride (lllllil) Nickel (mg/L) MW-24 Manganese (ug/L) (Class lll) Thallium (ug/L) Gross Alnlm (nCi/L) Sulfate (mwL) TDS (mg/L) Field pH (S.U.) MW-27 Nitrate+ Nitrite (as NJ (mg/L) (Class lfl) Fluoride (mg/L) Chloride (mg/L) MW-28 Selenium (uJ!/L) (Class lll) Nitrate+ Nitrite {as N} (ml!/Ll Uranium (ug/L) MW-29 Uranium (ug/L) (Clnss 111) MW-32 Chloride (mg/L) (Class Ill) Notes: NS= Not Required and Not Sampled NA= Not Applicable Exceedances are shown in yellow GWCLin Ql 2021 March 8, Sample 2021 Date GWDP 2.5 39.16 237 1/12/21 1309 2528 2976 1/11/21 0.62 70 58.31 1/14/21 3284.19 2.S 128 53.6 1/11/21 1918 9.82 5 993 2132 l/12/21 15 143 23.5 i 39 1/14/21 2 6.43 0.47 50 7507 ' 2.01 l/l4/2l 7.5 2903 4450 5.03 -8.5 5.6 l/14/21 0.85 105 11.l 1/15/21 5 4.9 15 1/15/21 35.39 1/14/21 Ql 2021 Results Fcbruar February March March 2021 2021 Q22021 Ql 2021 Monthly 2021 Monthly 2021 Sample Result Sample Monthly Sample Monthly Date Dute Result Date Result Rcquil'Cld Qu11rlcrly �ampling Wells 1.21 NA NA 46.4 46.4 185 2/9/21 254 3/8/21 221 04/20/21 1140 1260 1270 2010 2160 1950 2660 NS NA NS NA I 04/14/21 0.619 0.764 0.617 2200 1930 2190 57.4 2/10/2 I 3/9/21 04/21/21 71.3 63.9 3[00 2700 3060 17.7 14.3 17.0 184 189 192 2/10/2[ --3/9/21 56.3 04/14/21 - -I NA 10.2 17./ 14.3 17.4 /070 1130 1210 2-161} 2/9/21 2960 3/8/21 2400 04/13/21 19.7 22.2 20.2 354 380 388 Required Semiannual S.ompling Wells 25.0 35.l NS NA NS NA 4/20/21 2.75 NA NA 8.79 NA NA 0.916 NA NA 70.4 NA NA 7460 NA NA 2.74 NS NA NS NA 4/29/21 2.94 N1\ NA 2980 NA NA 4260 NA NA 5.08 NA NA 5.16 NS NA NS NA 4/15/21 NA 128 NA NA 14.0 NS NA NS NA 4/ l5/21 3.44 NA NA 10.3 NA NA 16.9 NS NA NS NA 4/!4/21 36.9 NS NA NS NA 4/13/21 Table 3-GWCL Exceedances under the March 8, 2021 GWDP Q2 2{121 Results = Q3 2021 Results Q4 2021 Results May2021 June2021 August August September September November November December December May2021 June 2021 Q32021 2021 Q42021 Q22021 Monthly Monthly Monthly Monthly Sample Q32021 Monthly 2021 2021 2021 Sample Q42021 2021 2021 2021 2021 Result Sample Result Sample Result Date Result Sample Monthly Monthly Monthly Date Result Monthly Monthly Monthly Monthly Date Date Date Result Sample Date Result Sample Date Result ompleDate Result Requireil Quarterly San1pling Wells Required Quurterly Snmpling Wells ·Required Quarterly �om'pling Wells 0.948 NA NA 0.924 NA NA 1.5 NA NA 47.7 46.4 52.1 48.3 57.0 49.6 52.8 53.6 53.9 237 5/10/21 NA 6/8/21 NA 7/27/21 376 8/l0/21 NA 9/7/21 NA l0/20/21 286 11/16/21 261 12/13/21 300 1290 1280 1270 1470 1370 1240 1360 1300 1350 2110 2190 1960 2680 NA NA 2200 2230 2140 2720 NS NA NS NA 7/28/21 3100 NS NA NS NA 10/20/21 2680 11/16/21 2920 I 2/14/21 2590 1.42 1.06 0.368 0.352 1.42 0.710 0.928 1.18 1.76 777 733 /590 723 996 516 540 568 1160 5/11/21 6/8/21 7/28/21 54.0 8/10/21 61.4 9/9/21 59.J I 0/21/21 55.2 11/16/21 56.9 I 2/15/21 57.5 69.6 54.9 75.9 2790 NA NA 3390 NA NA 30[0 3150 3130 17.7 18.6 17.0 20.6 16.5 15.4 14.3 /8.0 18.6 162 188 170 188 161 183 182 182 184 55.7 5/l 1/21 .'i8.3 6/8/21 54.l 7/29/21 56.3 8/9/21 56.1 9/8/21 60.4 10/19/21 54.6 11/17/21 53.6 12/14/21 58.8 1580 NA NA 2010 NA NA 1790 1710 1610 10.3 10.7 9.84 9.60 9.38 9.74 9.76 9.67 JO.I 18.6 18.9 20.6 18.7 15.7 /6.0 IS.I /9.3 17.9 1170 /200 1170 1210 1130 1130 1220 1180 ,no 2300 5/10/2[ 2610 6/7/21 2400 7/27/21 3100 8/9/21 2600 9/7/21 2870 10/19/21 2600 11/15121 2610 12/13/21 U20 20.1 21.7 20.8 20.0 19.3 20.2 20.9 21.S 21.8 377 384 374 391 365 356 371 366 376 Required Semiannual Sumpling Wells �cquircd Semiannual Sampling Wells Required Semiannual Sam_pling Wells 22.9 28.8 NS NA NS 22.2 NA 7/21/21 32.4 NS NA NS NA 11/9/21 23.1 26.4 NS NA NS NA 2.78 NA NA 2.71 NA NA 2.66 NA NA 8.08 NA NA 9.26 NA NA 9.30 NA NA 0.925 NA NA 1.4 NA NA 0.988 NA NA 72.4 NA NA 76.7 NA NA 76.7 NA NA 7540 NA NA 7890 NA NA 7430 NA NA 3.02 NS NA NS NA 7/29/21 2.9/ NS NA NS NA 11/10/21 3.14 NS NA NS NA 3.18 NA NA 1.92 NA NA 1.56 NA NA 2960 NA NA 3050 NA NA 3220 NA NA 4460 NA NA 4940 NA NA 4730 NA NA 5.00 NA NA 5,85 NA NA 5.23 NA NA 6.57 6.32 3.88 NS NA NS NA 7/22/21 NS NA NS NA 10/26/21 NS NA NS NA 0.69 NA 0.65 144 NA NA 152 NA NA 147 NA NA 13.4 NS NA NS NA 7/23/21 18.5 NS NA NS NA 10/26/21 11.2 NS NA NS NA 4,09 NA NA 6.09 NA NA 1.89 NA NA 8.52 NA NA 13.80 NA NA 6.03 NA NA 16.2 NS NA NS NA 7/22/21 15.8 NS NA NS NA l 0/27/21 14.9 NS NA '1 NS NA 31.8 NS NA NS NA 7/28/21 36.5 NS NA NS NA 11/2/21 36.1 NS NA NS NA -,, Table 3 G WCL Exceedances under the March 8 2021 GWDP Ql 2022 Results Q2 2022 Results Q3 2022 Results February February March 2022 March 2022 May 2022 May2022 June2022 June2022 August2022 August2022 September September Monitoring Well GWCL in March QI 2022 I QI 2022 2022 Monthly Q2 2022 Q22022 Monthly Q3 2022 Q32022 2022 2022 (Water Class) Constituent Exceeding GWCL 8,2021 GWDP Sample Date Result 2022 Monthly Monthly Sample Monthly Sample Date Result Monthly Monthly Sample Monthly Sample Date Result Monthly Monthly Monthly Monthly Sample Date Result Date Result Sample Date Result Date Result Sample Date Result Sample Date Result Required Quarterly Sampling Wells Re<Juircd Quarterly Sampling Wells Required Quurtedy Sampling Wells Nitrate+ Nitrite (as N) (mg/L) 2.5 2.55 NA NA 2.2 1.6 1.9 2.12 2.45 2.65 Chloride (mg/L) 39.16 51.1 57.2 67.7 54.9 59.5 46.4 54.0 67.4 68.1 MW-II Manganese (ug/L) 1/18/22 2/8/22 3/8/22 4/18/22 5/4/22 6/6/22 228 7/12/22 297 8/8/22 201 9/21/22 212 237 156 233 224 180 254 I (Class II) 866 1260 1300 Sulfate (111g/L) 1309 !020 1240 1170 1240 1270 1390 TDS (mg/L} 2528 2050 1900 2080 2060 2290 2360 2520 3230 2280 MW-25 (Class TDS (mg/L) 2976 1/17/22 2720 2/9/2022 2690 3/7/2022 2610 4/12/22 3600 Ill) 5/3/2022 2660 6/7/2022 2730 7/ 13/22 2830 8/9/2022 2780 9/20/2022 2750 I Nitrate+ Nitrite (OS N) (lllg/L) 0.62 0.601 0.367 0.600 0.8 1.1 0.60 1.63 1.56 0.491 MW-26 Chloroform (uQ/L) 70 818 1580 1460 4/20/22 447 5/4/22 616 6/7/22 /250 7/14/22 <1.0 8/9/22 1120 9/20/22 810 (Class Ill) Chloride (nw/Ll 58.31 l/20/22 77.1 2/9/22 58.6 3/8/22 64.l 56.8 63.2 47.4 61.0 65.0 62.1 TDS (mwL) 3284.19 3080 2980 2870 2560 2860 3120 3140 3120 NA Nit rate+ Nitrite (as N) (ml!/l,) 2.5 14.5 /3.6 16.6 17 15 11.0 17.6 13.5 /6.5 Chloride (mg/L) 128 181 184 196 173 195 126 108 185 182 MW-30 Selenium (Ul1/L) 53.6 1/17/22 56.7 2/9/22 57.7 3/7/22 62.0 4/20/22 64.9 5/4/22 69.4 6/7/22 65.7 7/13/22 61.l 8/9/22 64.3 9/20/22 70.0 (Class II) TDS (m}'./l.) 1918 1680 1640 1500 1400 1640 1660 1710 1580 NA Uranium (ug/L) 9.82 : I(), I 10.3 9.9 9.6 JO.I 9.6 10.0 10.J 8.3 Nitrate+ Nitrite (ns N) (mJ!/Ll 5 18.0 /3.5 17.0 18.0 13.0 13.0 /6.9 16.8 17.1 Sulfate (1111(/L) 993 1210 1250 731 1180 1220 1110 1260 1230 1200 MW-31 TDS (mg/L) 2132 l/19/22 2620 2/8/22 2680 3/7/22 2530 4/11/22 4300 5/3/22 2660 6/6/22 2690 7/12/22 2700 8/8/22 2700 9/20/22 2830 (Class Ill) Uranium (ug/L) 15 21.7 22.1 22.5 zz.o 22.9 21.5 22.6 22.7 18.8 Chloride (ml!IL) 143 370 379 416 372 381 351 421 396 390 Required SemiannualSnmpliog Wells Rc<111ired Semiannual Sampling Wells Re<1uired Semiannual Sampling Wells MW-12 Uranium (ug/L�) 23.5 22. l 20.5 21.6 l/20/22 NS NA NS NA 4/19/22 NS NA NS NA 7/14/22 NS NA NS NA (Class lll) Selenium (ug/L) 39 25.6 31.3 29.2 Beryllium (ug/L) 2 2.71 NA NA 2.5 NA NA 2.7 NA NA Cadmium (ug/L) 6.43 8.46 NA NA 9.20 NA NA 8.6 NA NA Fluoride (mj!/L} 0.47 I I NA NA 0.8 NA NA 0.760 NA NA Nickel (mg/LJ 5() i 80.9 NA NA 74.3 NA NA 69.9 NA NA MW-24 Manganese (ug/L) 7507 7630 NA NA 7070 NA NA 7/20/22 7540 NA NA (Class Ill) Thallium (u_g/L) 2.01 l/27/22 2.66 NS NA NS NA 4/27/22 3.1 NS NA NS NA 7/28/22 3.0 NS NA NS NA Gross Aloha (oCi/U 7.5 2.26 NA NA 2.28 NA NA 2.55 NA NA Sulfate (nu!/L) 290'.l 3()60 NA NA 3120 NA NA 2800 NA NA TDS (me/I.) 4450 4140 NA NA 3350 NA NA 4200 NA NA Field pH (S.U.) 5.03 - 8.5 5.31 NA NA 4.81 NA NA 4.89 NA NA 4.80 MW-27 Nitrate+ Nitrite (as NJ (mg/L) 5.6 6.25 6.30 5.18 (Class lll) 1/18/22 NS NA NS NA 4/12/22 NS NA NS NA 7/15/22 NS NA NS NA Fluoride (mg/L) 0.85 NA 0.90 0.530 --Chloride (mg/L) 105 140 NA NA 130 NA NA 159 NA NA MW-28 Selenium (ue/1.) II.I I /20/22 13.3 NS NA NS NA 4/19/22 19.8 NS NA NS NA 7/15/22 20.8 NS NA NS NA (Class Ill) Nitrate+ Nitrite (as N) (mg/L) 5 4.03 NA NA 5.1 NA NA 5.16 NA NA Uranium (u,uL) 4.9 8.50 NA NA JO.JO NA NA 12.4 NA NA MW-29 Uranium (ug/L) !Class 1111 15 1/18/22 15.1 NS NA NS NA 4/14/22 /5.7 NS NA NS NA 7/14/22 15.1 NS NA NS NA MW-32 Chloride {mg/L) 35.39 1/19/22 35.0 NS NA NS NA 4/11/22 (Class Ill)28.6 NS NA NS NA 7/ 15/22 28.2 NS NA NS NA Purs.ua.ntto the DWM�C letter Qf August 8, 2022, these c111nstltllentsWIII no longer be monitored on an acce(erated'sehedtile. These _t::ortstltuen\sWIII be dropped from this report after this quarter. INDEX OFT ABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab Cl Field Data Worksheets Accelerated Monitoring, August 2022 Tab C2 Field Data Worksheets Accelerated Monitoring, September 2022 Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports -Quarterly Sampling Tab F Laboratory Analytical Reports -Accelerated Monitoring Tab Fl Laboratory Analytical Reports -Accelerated Monitoring, August 2022 Tab F2 Laboratory Analytical Reports -Accelerated Monitoring, September 2022 Tab G Quality Assurance and Data Validation Tables G-lA/B G-2A/B G-3A/B G-4A/B G-5AIB G-6AIB G-7A/B G-8 A/B G-9A/B Field Data QNQC Evaluation Holding Time Evaluation Laboratory Temperature Check Analytical Method Check Reporting Limit Evaluation Trip Blank Evaluation QNQC Evaluation for Sample Duplicates Radiologies Counting Error Laboratory Matrix QC Tab H Kriged Current Quarterly Groundwater Contour Map Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter MW-41 perched monitoring well installed July, 2022 TW4-43 temporary perched monitoring well � installed September, 2021 TWN-20 temporary perched nitrate monitoring C well installed April, 2021 MW-24A perched monitoring well installed •December 2019 TW4-42 temporary perched monitoring well ¢ installed April 2019 TW4-40 perched chloroform pumping well EB installed February 2018 TW4-19 perched chloroform or EB nitrate pumping well MW-38 perched monitoring well installed February 2018 MW-5 •perched monitoring well TW4-12 temporary perched monitoring well TWN-7 temporary perched nitrate monitoring � well PIEZ-1 perched piezometer r.l RUIN SPRING b seep or spring DR-10 DfU1 DR-12 • MW..JA HYDRO GEO CHEM,INC. MW-28 a o TWN•20"1WN-07 Celi 2 • MW� WHITE MESA SITE PLAN SHOWING LOCATIONS OF PERCHED WELLS AND PIEZOMETERS APPROVED DATE REFERENCE FIGURE H:/718000/may22/Uwelloc0922.srf A-1 Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 7/12/2022 11:17 7/12/2022 11:18 7/12/2022 11:19 7/12/2022 11:20 !volume of water purged (gals) I Final Depth to Water (feet) 57.93 58.15 58.37 58.59 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-11 Sampling Program MW-11 07122022 Sampling Event 2022 Q3 GW 7/12/2022 6:50 7/12/2022 11:20 !sampler I TH/DL Pump Weather Conditions Sunny QED External Ambient Temperature (C) 23 2 Casings Previous Well Sampled MW-31 29.18 269.02 7.0 Well Depth (ft) 130.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 85.30 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3181 7.55 15.15 356 98.0 4.3 3185 7.53 15.13 353 105.0 4.0 3190 7.53 15.12 350 107.0 4.0 3184 7.52 15.10 347 110.0 4.2 Pumping Rate Calculations 58.59 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 270.00 86.95 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE u 4 Deg C y y WATER 1 250-ml HOPE y HN03 (pH<2) y y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u H2504 (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u 4 Deg C y y WATER 1 250-ml HOPE y HN03 y Arrived on site at 0647. Purge began at 0650. Purged well for a total 270 minutes. Purge ended and samples collected at 1120. Water was mostly clear with tiny little bubbles surfacing. Left site at 1130. Signature of Field Technician -2)(L_,�.+,;1:;4":4, I Location ID Field Sample ID Purge Date & Time Sample Date & Time -Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7 .0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 7/14/2022 12:37 7/14/2022 12:38 7/14/2022 12:39 7/14/2022 12:40 !Volume of water purged (gals) I Final Depth to Water (feet) 27.55 27.77 27.99 28.21 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Heavy Metals - U and Se only Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-12 Sampling Program MW-12 07142022 Sampling Event 7/14/2022 10:30 7/14/2022 12:40 I sampler Pump Weather Conditions QED External Ambient Temperature (C) 2 Casings Previous Well Sampled 13.60 125.36 7.0 Well Depth (ft) 4.0 Well Casing Diameter (in) 1000 Depth to Water Before Purging (ft) Conductivity (um hos/cm) pH (pH Units) Temp (deg C)Redox (mV)Turbidity (NTU) 4140 6.90 15.67 250 0 4158 6.88 15.67 251 0 4165 6.87 15.72 252 0 4163 6.87 15.73 253 0 Pumping Rate Calculations 28.21 Flow Rate (Q = S/60) (gal/min) Time to evacuate 2 Casing Volumes (min) 122.37 Number of casing Volumes Volume, if well evacuated to dryness () Sample Container Collected? Matrix Number I Type Sample Filtered? Type y WATER 1 I 250-ml HOPE y HN03 (pH<2) 2022 Q3 GW TH/DL Partly cloudy 27 MW-29 130.40 4 109.57 Dissolved Oxygen(%) Before/After 30.0 30.3 31.0 31.4 .217 130.00 2.00 0 Preservative I Added? I y I Arrived on site at 1027. Purge began at 1030. Purged well for a total of 130 minutes. Purge ended and samples collected at 1240. Water was clear. Left site at 1242. Signature of Field Technician Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7 .0 pH Buffer 4.0 Specific Conductance (micromhos) DatefTime Gallons Purged (gal) 7/13/2022 13:42 7/13/2022 13:43 7/13/2022 13:44 7/13/2022 13:45 !Volume of water purged (gals) I Final Depth to Water (feet) 38.40 38.62 38.84 39.06 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals - Full Suite VOCs - Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-14 Sampling Program MW-14 07132022 Sampling Event 2022 Q3 GW 7/13/2022 10:45 7/13/2022 13:45 !sampler TH/DL Pump Weather Conditions Sunny QED External Ambient Temperature (C)28 2 Casings Previous Well Sampled MW-25 17.61 162.37 7.0 Well Depth (ft) 128.70 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 101.72 conduct1v1ty DISSOived (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3902 6.76 13.25 324 1.4 1.2 3906 6.74 15.40 324 1.4 1.1 3898 6.72 14.38 324 1.4 1.1 3894 6.72 15.30 324 1.5 1.1 Pumping Rate Calculations 39.06 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 180.00 102.95 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE u 4 DegC y y WATER 1 250-ml HOPE y HN03 (pH<2) y y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u 4 OegC y y WATER 1 250-ml HOPE y HN03 y !Arrived on site at 1042. Purge began at 1045. Purged well for a total of 180 minutes. Purge ended and samples collected at 1345. Water was clear. Left site at 1355. Signature of Field Technician �LV ��+-Ad�) Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-24 Sampling Program Field Sample ID MW-24 07202022 Sampling Event 2022 Q3 GW Purge Date & Time 7/19/2022 7:15 Sample Date & Time 7/20/2022 8:10 !sampler I TH/DL I Purging Equipment Bailer Weather Conditions Sunny Pump Type Grundfos External Ambient Temperature (C)21 Purging Method 2 Casings Previous Well Sampled MW-24A Casing Volume (gal) 6.85 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 120.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 109.50 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 7/19/2022 7:23 5.00 4484 4.90 15.12 552 73.0 81.0 7/20/2022 8:10 4475 4.88 16.50 Before 7/20/2022 8:14 4477 4.89 16.38 After Pumping Rate Calculations I Volume of water purged (gals)14.00 Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () I Final Depth to Water (feet)119.95 Number of casing Volumes 2.00 Volume, if well evacuated to dryness (gals) 14.00 Name of Certified Analytical Laboratory GEL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Gross Alpha y WATER 1 250-ml HDPE y HNO3 y Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HNO3 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 DegC y Comments: Arrived on site at 0711. Purge began at 0715. Bailed a total of 14 gallons rom well. Bailed well dry. Water was dirty. Left site at 0739. Arrive on site at 0805. Depth to water was 109.55. Samples bailed and collected at 0810. Left site at 0815. Signature of Field Technician �--'-'--f--/-��, Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 7/27/2022 13:20 7/28/2022 6:59 7/28/2022 7:03 !Volume of water purged (gals) I Final Depth to Water (feet) 14.40 Name of Certified Analytical Laboratory GEL Analytical Samples Information Type of Sample/Analysis Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-24 Sampling Program MW-24 07282022 Sampling Event 2022 GW MW-24Resamp -Rev 1 7/27/2022 12:05 7/28/2022 7:00 !Sampler TH/DL Pump Weather Conditions Cloudy QED External Ambient Temperature (C)25 2 Casings Previous Well Sampled N/A 6.94 72.30 7.0 Well Depth (ft) 120.00 4.0 Well Casing Diameter (in)4 1000 Depth to Water Before Purging (ft) 109.37 Conductivity Dissolved (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3436 4.89 16.18 425 1.1 92.0 4476 4.78 16.20 Before 4483 4.80 16.15 After Pumping Rate Calculations 14.40 Flow Rate (Q = S/60) (gal/min).192 Time to evacuate 2 Casing Volumes (min) 75.00 118.93 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () Sample Container Preservative Collected? Matrix Number I Type Sample Filtered? Type I Added? y WATER 1 I 250-ml HDPE y HN03 I y Arrived on site at 1200. Purge began at 1205. Purged well for a total of 75 minutes. Purged well dry. Purge ended at 1320. Water was clear. Left site at 1323. Arrived on site at 0655. Depth to water was 109.37. Samples collected at 0700. Left site at 0704. Signature of Field Technician Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 7/18/2022 13:20 7/19/2022 7:00 7/19/2022 7:10 !Volume of water purged (gals) I Final Depth to Water (feet) 15.36 Name of Certified Analytical Laboratory GEL Analytical Samples Information Type of Sample/Analysis Gross Alpha Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganics Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-24A Sampling Program MW-24A 07192022 Sampling Event 2022 Q3 GW 7/18/2022 12:00 7/19/2022 7:00 !Sampler I TH/DL Pump Weather Conditions Sunny QED External Ambient Temperature (C)30 2 Casings Previous Well Sampled MW-28 7.45 77.67 7.0 Well Depth (ft) 122.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 110.58 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4353 4.98 15.36 425 3.6 97.2 4431 4.88 15.75 Before 4446 4.90 15.70 After Pumping Rate Calculations 15.36 Flow Rate (Q = S/60) (gal/min) .192 Time to evacuate 2 Casing Volumes (min) 80.00 120.03 Number of casing Volumes 2.00 Volume, if well evacuated to dryness (gals) 15.36 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HDPE y HNO3 y y WATER 1 250-ml HDPE u 4 Deg C y y WATER 1 250-ml HDPE y HNO3 (pH<2) y y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y y WATER 1 250-ml HDPE u 4 Deg C y Arrived on site at 1156. Purge began at 1200. Purged well for a total of 80 minutes. Purged well dry. Purge ended at 1320. Water was clear. Left site at 1321. Arrived on site at 0655. Depth to water was 110.58. Samples collected at 0700. Left site at 0711. Signature of Field Technician ..:3�-�-1-/2--{L� I Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date!Time Gallons Purged (gal) 7/13/2022 10:57 7/13/2022 10:58 7/13/2022 10:59 7/13/2022 11:00 !Volume of water purged (gals) I Final Depth to Water (feet) 44.91 45.13 45.35 45.57 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals - Full Suite VOCs - Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-25 Sampling Program MW-25 07132022 Sampling Event 2022 Q3 GW 7/13/2022 7:30 7/13/2022 11:00 I Sampler TH/OL Pump Weather Conditions Sunny QED External Ambient Temperature (C) 23 2 Casings Previous Well Sampled MW-30 21.53 198.48 7.0 Well Depth (ft) 115.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 82.02 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3179 7.04 15.51 362 2.4 4.8 3181 7.00 15.31 362 2.0 4.6 3185 6.99 15.25 361 2.1 4.5 3190 6.98 15.16 361 2.0 4.6 Pumping Rate Calculations 45.57 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 84.67 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE u 4 DegC y y WATER 1 250-ml HOPE y HN03 (pH<2) y y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u 4Deg C y y WATER 1 250-ml HOPE y HN03 y I Arrived on site at 0727. Purge began at 0730. Purged well for a total of 21 O minutes. Purge ended and samples collected at 1100. Water was clear. Left site at 1110. Signature of Field Technician �,,,,.�+-/2--�:4, Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration () pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged 7/14/2022 7:59 !Volume of water purged O I Final Depth to Water (feet) Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-26 Sampling Program MW-26 07142022 Sampling Event 2022 Q3 GW 7/14/2022 8:00 7/14/2022 8:00 I sampler TH/DL Pump Weather Conditions Sunny Grundfos External Ambient Temperature (C) 23 2 Casings Previous Well Sampled MW-40 29.28 7.0 Well Depth (ft) 121.33 4.0 Well Casing Diameter (in)4 1000 Depth to Water Before Purging (ft) 76.48 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3469 7.20 16.50 317 0 41.4 Pumping Rate Calculations Flow Rate (Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes () 103.41 Number of casing Volumes Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE u 4 Deg C y y WATER 1 250-ml HOPE y HN03 (pH<2) y y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-mL HOPE u 4 Deg C y y WATER 1 250-ml HOPE y HN03 y I Arrived on site at 0755. Samples collected at 0800. Water was clear. Left site at 0807. Signature of Field Technician �-•; ,, . .,. -<---f--/ -a'� Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 7/15/2022 10:42 7/15/2022 10:43 7/15/2022 10:44 7/15/2022 10:45 !Volume of water purged (gals) I Final Depth to Water (feet) 49.25 49.47 49.69 49.91 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Nitrate/nitrite as N Fluoride Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-27 Sampling Program MW-27 07152022 Sampling Event 2022 Q3 GW 7/15/2022 6:55 7/15/2022 10:45 I sampler TH/DL Pump Weather Conditions Cloudy QED External Ambient Temperature (C)21 2 Casings Previous Well Sampled MW-12 23.73 218.70 7.0 Well Depth (ft) 95.00 4.0 Well Casing Diameter (in)4 1000 Depth to Water Before Purging (ft)58.66 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 1211 7.70 15.90 316 0 96.0 1212 7.69 15.92 315 0 97.0 1220 7.69 15.70 314 0 97.0 1202 7.69 15.67 314 0 97.3 Pumping Rate Calculations 49.91 Flow Rate (0 = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 230.00 60.27 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u None N I Arrived on site at 0650. Purge began at 0655. Purged well for a total of 230 minutes. Purge ended and samples collected at 1045. Water was clear. Left site at 1048. Signature of Field Technician Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-28 Sampling Program Field Sample ID MW-28_07152022 Sampling Event 2022 Q3 GW Purge Date & Time 7/15/2022 11:00 Sample Date & Time 7/15/2022 14:35 !sampler TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type Grundfos External Ambient Temperature (C)28 Purging Method 2 Casings Previous Well Sampled MW-32 Casing Volume (gal) 23.08 Calculated Casing Volumes Purge Duration (min) 212.75 pH Buffer 7.0 7.0 Well Depth (ft) 110.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 74.65 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 7/15/2022 14:32 46.00 4220 6.72 16.00 297 2.2 33.0 7/15/2022 14:33 46.22 4229 6.71 15.93 296 2.1 34.2 7/15/2022 14:34 46.43 4239 6.71 15.85 296 2.0 34.9 7/15/2022 14:35 46.65 4230 6.70 15.79 295 2.0 34.5 Pumping Rate Calculations I Volume of water purged (gals)46.65 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 215.00 I Final Depth to Water (feet)77.65 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytic-al Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Heavy Metals - U and Se only y WATER 1 250-ml HOPE y HNO3 (pH<2) y Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2SO4 (pH<2), 4 Deg C y Comments: I Arrived on site at 1057. Purge began at 1100. Purged well for a total of 215 minutes. Purge ended and samples collected at 1435. Water was clear. Left site at 1440. Signature of Field Technician 2),,, ·A--.',;✓� Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7 .0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 7/14/2022 13:17 7/14/2022 13:18 7/14/2022 13:19 7/14/2022 13:20 !Volume of water purged (gals} I Final Depth to Water (feet) 38.40 38.62 38.84 39.06 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Heavy Metals - U only Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-29 Sampling Program MW-29 07142022 Sampling Event 2022 Q3 GW 7/14/2022 10:20 7/14/202213:20 !Sampler TH/DL Pump Weather Conditions Partly cloudy QED External Ambient Temperature (C)27 2 Casings Previous Well Sampled MW-26 18.27 168.39 7.0 Well Depth (ft) 135.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 107.02 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity {NTU) Oxygen(%) Before/After 4549 6.68 15.69 224 12.1 1.3 4550 6.66 15.79 223 13.0 1.1 4501 6.65 15.75 222 14.0 1.2 4540 6.64 15.65 221 13.0 1.1 Pumping Rate Calculations 39.06 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 180.00 109.55 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number I Type Sample Filtered? Type I Added? y WATER 1 I 250-ml HDPE y HNO3 (pH<2) I y I Arrived on site at 1015. Purge began at 1020. Purged well for a total of 180 minutes. Purge ended and sample collected at 1320. Water was clear. Left site at 1322. Signature of Field Technician Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7 .0 pH Buffer 4.0 Specific Conductance (micromhos) DatefTime Gallons Purged (gal) 7/13/2022 10:32 7/13/2022 10:33 7/13/2022 10:34 7/13/2022 10:35 !Volume of water purged (gals) !Final Depth to Water (feet) 44.91 45.13 45.35 45.57 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganlcs Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-30 Sampling Program MW-30 07132022 Sampling Event 2022 Q3 GW 7/13/2022 7:05 7/13/2022 10:35 Sampler TH/DL Pump Weather Conditions Sunny QED External Ambient Temperature (C) 22 2 Casings Previous Well Sampled MW-11 22.60 208.35 7.0 Well Depth (ft) 110.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 75.38 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox(mV) Turbidity (NTU) Oxygen(%) Before/After 2236 7.38 15.21 368 0 54.0 2232 7.35 15.10 366 0 53.0 2238 7.33 15.06 365 0 52.0 2237 7.33 15.00 364 0 52.5 Pumping Rate Calculations 45.57 Flow Rate (Q = S/60) (gal/min).217 Time to evacuate 2 Casing Volumes (min) 210.00 76.98 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HDPE u 4 DegC y y WATER 1 250-ml HDPE y HN03 (pH<2) y y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u 4 Deg C y y WATER 1 250-ml HOPE y HN03 y I Arrived on site at 0700. Purge began at 0705. Purged well for a total of 21 O minutes. Purge ended and samples collected at 1035. Water was clear. Left site at 1045. Signature of Field Technician �u,�r��+-/•�4, Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 7/12/2022 12 :42 7/12/2022 12:43 7/12/2022 12:44 7/12/2022 12:45 !Volume of water purged (gals) I Final Depth to Water (feet) 78.55 78.77 78.98 79.20 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-31 Sampling Program MW-31 07122022 Sampling Event 2022 Q3 GW 7/12/2022 6:40 7/12/2022 12:45 !sampler I TH/DL Pump Weather Conditions Sunny QED External Ambient Temperature (C)23 2 Casings Previous Well Sampled N/A 39.40 363.21 7.0 Well Depth (ft) 130.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 69.65 Conductivity Dissolved (umhos/cm) pH {pH Units) Temp(deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3300 7.34 15.55 339 0 114.0 3387 7.31 15.48 338 0 115.0 3418 7.30 15.45 338 0 115.0 3440 7.28 15.43 337 0 115.0 Pumping Rate Calculations 79.20 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 365.00 72.87 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE u 4 DegC y y WATER 1 250-ml HDPE y HN03 (pH<2) y y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u H2504 (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u 4 Deg C y y WATER 1 250-ml HOPE y HN03 y j Arrived on site at 0635. Purge began at 0640. Purged well for a total of 365 minutes. Purge ended and samples collected at 1245. Water was clear. Left site at 1255. Signature of Field Technician � '4> u,.•---�J:-«� I Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7 .0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 7/15/2022 12:17 7/15/2022 12:18 7/15/2022 12:19 7/15/2022 12:20 !Volume of water purged (gals) !Final Depth to Water (feet) 64.44 64.66 64.88 65.10 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Chloride Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-32 Sampling Program MW-32 07152022 Sampling Event 7/15/2022 7:20 7/15/2022 12:20 !sampler I Pump Weather Conditions QED External Ambient Temperature (C) 2 Casings Previous Well Sampled 31.14 287.07 7.0 Well Depth (ft) 4.0 Well Casing Diameter (in) 1000 Depth to Water Before Purging (ft) Conductivity (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) 3677 6.71 15.55 215 4.9 3734 6.69 15.45 216 5.1 3724 6.67 15.44 216 5.2 3722 6.65 15.43 216 5.2 Pumping Rate Calculations 65.10 Flow Rate (Q = S/60) (gal/min) Time to evacuate 2 Casing Volumes (min) 86.97 Number of casing Volumes Volume, if well evacuated to dryness () Sample Container Collected? Matrix Number I Type Sample Filtered? Type y WATER 1 I 500-ml Poly u None 2022 Q3 GW TH/DL Cloudy 22 MW-27 130.60 4 82.90 Dissolved Oxygen(%) Before/After 6.9 6.8 6.9 6.8 .217 300.00 2.00 0 Preservative I Added? I N I Arrived on site at 0715. Purge began at 0720. Purged well for a total of 300 minutes. Purge ended and samples collected at 1220. Water was a little murky. Left site at 1222. Signature of Field Technician I Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 7/13/2022 12:27 7/13/2022 12:28 7/13/2022 12:29 7/13/2022 12:30 !Volume of water purged (gals) I Final Depth to Water (feet) 14.53 14.75 14.97 15.19 Name of Certified Analytical Laboratory GEL Analytical Samples Information Type of Sample/Analysis Gross Alpha Total Dissolved Soilds Heavy Metals -Full Suite VOCs - Full Suite for GW Nutrients General lnorganics Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-36 MW-36 07132022 7/13/2022 11:20 7/13/2022 12:30 Pump QED 2 Casings 7.21 66.50 7.0 4.0 1000 Conductivity (umhos/cm) 4747 4821 4763 4841 15.19 111.43 Sample Collected? Matrix y WATER y WATER y WATER y WATER y WATER y WATER Sampling Program Sampling Event !sampler Weather Conditions External Ambient Temperature (C) Previous Well Sampled Well Depth (ft) Well Casing Diameter (in) Depth to Water Before Purging (ft) pH (pH Units) Temp (deg C) Redox (mV) 7.15 15.76 352 7.14 15.70 351 7.12 15.70 351 7.11 15.74 350 Pumping Rate Calculations Flow Rate (Q = S/60) (gal/min) Time to evacuate 2 Casing Volumes (min) Number of casing Volumes Volume, if well evacuated to dryness () Container Number Type Sample Filtered? 1 250-ml HOPE y 1 250-mL HOPE u 1 250-mL HOPE y 3 40mlVOA u 1 250-mL HOPE u 1 250-mL HOPE u 2022 Q3 GW TH/DL Sunny 28 MW-14 121.60 4 110.55 Dissolved Turbidity (NTU) Oxygen(%) Before/After 1.0 76.0 1.0 80.0 1.0 81.0 1.0 83.0 .217 70.00 2.00 0 Preservative Type Added? HN03 y 4 Deg C y HN03 (pH<2) y HCI (pH<2), 4 Deg C y H2S04 (pH<2}, 4 Deg C y 4 Deg C y I Arrived on site at 1115. Purge began at 1120. Purged well for a total of 70 minutes. Purge ended and samples collected at 1230. Water was clear. Left site at 1240. Signature of Field Technician -2> ,,. -_c.--,'.-�4, Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration () pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date!Time Gallons Purged (gal) 7/19/2022 8:04 7/20/2022 8:30 7/20/2022 8:38 !Volume of water purged (gals) j Final Depth to Water (feet) 5.00 Name of Certified Analytical Laboratory GEL Analytical Samples Information Type of Sample/Analysis Gross Alpha Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganics Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-38 Sampling Program MW-38 07202022 Sampling Event 2022 Q3 GW 7/19/2022 8:00 7/20/2022 8:30 !sampler TH/DL Bailer Weather Conditions Sunny Grundfos External Ambient Temperature (C)23 2 Casings Previous Well Sampled MW-24 2.73 7.0 Well Depth (ft) 74.40 4.0 Well Casing Diameter (in} 4 1000 Depth to Water Before Purging (ft) 70.21 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4325 6.04 15.86 526 65.0 105.0 4300 6.70 16.50 Before 4297 6.71 16.40 After Pumping Rate Calculations 5.00 Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () 74.31 Number of casing Volumes 1.82 Volume, if well evacuated to dryness (gals) 5.00 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE y HN03 y y WATER 1 250-ml HOPE u 4 DegC y y WATER 1 250-ml HOPE y HN03 (pH<2) y y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u 4 DegC y Arrived on site at 0755. Bailing began at 0800. Bailed a total of 5 gallons from well. Bailed well dry. Water started clear and ended murky. Bailing ended at 0804. Left site at 0807. Arrived on site at 0825. Depth to water was 70.25. Samples bailed and collected at 0830. Left site at 0840. Signature of Field Technician � �, c,,.e.-,.--1-:/-:%� Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 7/14/2022 9:32 7/14/2022 9:33 7/14/2022 9:34 7/14/2022 9:35 !Volume of water purged (gals) I Final Depth to Water (feet) 49.25 49.47 49.69 49.91 Name of Certified Analytical Laboratory GEL Analytical Samples Information Type of Sample/Analysis Gross Alpha Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganics Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-39 Sampling Program MW-39 07142022 Sampling Event 2022 Q3 GW 7/14/2022 5:45 7/14/2022 9:35 I sampler I TH/DL Pump Weather Conditions Partly cloudy QED External Ambient Temperature (C) 20 2 Casings Previous Well Sampled MW-36 24.78 228.39 7.0 Well Depth (ft) 102.50 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 64.55 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4812 4.40 15.40 368 0 4.1 4800 4.35 15.37 408 0 4.0 4810 4.30 15.35 422 0 4.0 4811 4.28 15.34 434 0 4.0 Pumping Rate Calculations 49.91 Flow Rate (Q = S/60) (gal/min).217 Time to evacuate 2 Casing Volumes (min) 230.00 67.94 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE y HN03 y y WATER 1 250-ml HOPE u 4 DegC y y WATER 1 250-ml HOPE y HN03 (pH<2) y y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u 4 DegC y I Arrived on site at 0542. Purge began at 0545. Purged well for a total of 230 minutes. Purge ended and samples collected at 0935. Water was clear. Left site at 0945. Signature of Field Technician I I I <:-� !._��� -.;;;;;-,-�,,.. ..... -:z :5 Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) DatefTime Gallons Purged (gal) 7/14/2022 9:57 7/14/2022 9:58 7/14/2022 9:59 7/14/2022 10:00 !Volume of water purged (gals) I Final Depth to Water (feet) 52.51 52.73 52.94 53.16 Name of Certified Analytical Laboratory GEL Analytical Samples Information Type of Sample/Analysis Gross Alpha Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganics Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-40 Sampling Program MW-40 07142022 Sampling Event 2022 Q3 GW 7/14/2022 5:55 7/14/2022 10:00 !sampler I TH/DL Pump Weather Conditions Partly cloudy QED External Ambient Temperature (C)20 2 Casings Previous Well Sampled MW-39 26.21 241.64 7.0 Well Depth (ft) 120.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 79.85 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3870 7.28 15.31 250 0 109.0 3877 7.22 15.33 253 0 107.0 3880 7.18 15.25 256 0 106.3 3890 7.17 15.23 259 0 106.7 Pumping Rate Calculations 53.16 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 245.00 80.78 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-mL HDPE y HNO3 y y WATER 1 250-mL HDPE u 4 Deg C y y WATER 1 250-mL HDPE y HNO3 (pH<2) y y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y y WATER 1 250-mL HDPE u H2SO4 (pH<2), 4 Deg C y y WATER 1 250-mL HDPE u 4 DegC y I Arrived on site at 0552. Purge began at 0555. Purged well for a total of 245 minutes. Purge ended and samples collected at 1000. Water was clear. Left site at 1010. Signature of Field Technician I Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume O Calculated Casing Volumes Purge Duration () pH Buffer 7 .0 pH Buffer 4.0 Specific Conductance O Dateffime !Volume of water purged () I Final Depth to Water (feet) Gallons Purged Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/ Analysis Total Dissolved Soilds Heavy Metals -Full Suite VOCs - Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: I Duplicate of MW-38 Signature of Field Technician Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-65 Sampling Program MW-65 07202022 Sampling Event 2022 Q3 GW 7/20/2022 8:30 !sampler TH/DL Weather Conditions External Ambient Temperature O Previous Well Sampled Well Depth (ft) Well Casing Diameter () Depth to Water Before Purging (ft) Conductivity pH Temp Redox Turbidity Dissolved Oxygen I Before/After I Pumping Rate Calculations Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () Number of casing Volumes Volume, if well evacuated to dryness() Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE u 4 Deg C y y WATER 1 250-ml HOPE y HN03 (pH<2) y y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u 4 Deg C y y WATER 1 250-ml HOPE y HN03 y Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7 .0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 8/8/2022 12:42 8/8/2022 12:43 8/8/2022 12:44 8/8/2022 12:45 !Volume of water purged (gals) I Final Depth to Water (feet) 57.93 58.15 58.37 58.59 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Chloride Heavy Metals -Mn only Sulfate Total Dissolved Soilds Nitrate/nitrite as N Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-11 Sampling Program MW-11 08082022 Sampling Event August Monthly 8/8/2022 8:15 8/8/2022 12:45 !sampler I TH/DL Pump Weather Conditions Sunny QED External Ambient Temperature (C)22 2 Casings Previous Well Sampled MW-31 29.15 268.72 7.0 Well Depth (ft) 130.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 85.35 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3091 7.55 15.43 312 111.0 5.1 3087 7.60 15.15 310 120.0 4.2 3060 7.61 15.10 308 126.0 4.0 3059 7.61 15.19 307 127.0 3.9 Pumping Rate Calculations 58.59 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 270.00 85.52 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 500-ml Poly u None N y WATER 1 250-ml HDPE y HNO3 (pH<2) y y WATER 1 250-ml HDPE u None N y WATER 1 250-ml HDPE u 4 Deg C y y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y Arrived on site at 0810. Purge began at 0815. Purged well for a total of 270 minutes. Purge ended and samples collected at 1245. Water was mostly clear but had tiny little bubbles surfacing. Left site at 1353. Signature of Field Technician � ,,, .,,.___--✓-L"� I Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7 .0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 8/9/2022 11:02 8/9/2022 11:03 8/9/2022 11:04 8/9/2022 11:05 !Volume of water purged (gals) I Final Depth to Water (feet) 44.91 45.13 45.35 45.57 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-25 Sampling Program MW-25 08092022 Sampling Event August Monthly 8/9/2022 7:35 8/9/2022 11:05 !Sampler TH/DL Pump Weather Conditions Partly cloudy QED External Ambient Temperature (C)21 2 Casings Previous Well Sampled MW-30 21.53 198.48 7.0 Well Depth (ft) 115.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 82.02 Conductivity Dissolved (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3162 7.12 15.80 314 0 3.4 3139 7.09 15.84 314 0 3.5 3145 7.07 15.72 313 1.0 3.4 3149 7.06 15.70 313 1.0 3.4 Pumping Rate Calculations 45.57 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 83.88 Number of casing Volumes 2.00 Volume, if well evacuated to dryness (} 0 Sample Container Preservative Collected? Matrix Number I Type Sample Filtered? Type I Added? y WATER 1 I 250-ml HOPE u 4 DegC I y I Arrived on site at 0730. Purge began at 0735. Purged well for a total of 21 O minutes. Purge ended and sample collected at 1105. Water was clear. Left site at 1107. Signature of Field Technician Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration () pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) DatefTime 8/9/2022 13:00 !Volume of water purged () I Final Depth to Water (feet) Gallons Purged Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Chloride Nitrate/nitrite as N Total Dissolved Soilds VOCs-Chloroform Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-26 Sampling Program MW-26 08092022 Sampling Event August Monthly 8/9/2022 13:00 8/9/2022 13:00 !sampler TH/DL Pump Weather Conditions Sunny Grundfos External Ambient Temperature (C)30 2 Casings Previous Well Sampled MW-25 28.73 7.0 Well Depth (ft) 121.33 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 77.32 Conductivity Dissolved (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3462 7.02 18.2 254 2.0 35.0 Pumping Rate Calculations Flow Rate (Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes () 97.68 Number of casing Volumes Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 500-mL Poly u None N y WATER 1 250-mL HDPE u H2504 (pH<2), 4 Deg C y y WATER 1 250-mL HOPE u 4DegC y y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y I Arrived on site at 1256. Samples collected at 1300. Water was clear. Left site at 1305. Signature of Field Technician Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 8/9/2022 10:47 8/9/2022 10:48 8/9/2022 10:49 8/9/2022 10:50 !Volume of water purged (gals) I Final Depth to Water (feet) 44.91 45.13 45.35 45.57 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Chloride Nitrate/nitrite as N Heavy Metals - U and Se only Total Dissolved Soilds Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-30 Sampling Program MW-30 08092022 Sampling Event August Monthly 8/9/2022 7:20 8/9/2022 10:50 !Sampler TH/DL Pump Weather Conditions Partly cloudy QED External Ambient Temperature (C)20 2 Casings Previous Well Sampled MW-11 22.59 208.23 7.0 Well Depth (ft) 110.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 75.40 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 2230 7.37 15.50 307 0 53.0 2242 7.35 15.55 306 0 55.0 2234 7.34 15.49 306 0 54.0 2230 7.33 15.48 306 0 54.0 Pumping Rate Calculations 45.57 Flow Rate (Q = S/60) (gaVmin) .217 Time to evacuate 2 Casing Volumes (min) 210.00 77.90 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? V WATER 1 500-mL Poly u None N y WATER 1 250-mL HDPE u H2SO4 (pH<2), 4 Deg C y y WATER 1 250-ml HDPE y HN03 (pH<2) y y WATER 1 250-ml HDPE u 4 Deg C y I Arrived on site at 0715. Purge began at 0720. Purged well for a total of 210 minutes. Purge ended and samples collected at 1050. Water was clear. Left site at 1100. Signature of Field Technician �--', tJU_,,c_�-1-/:�4� Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-31 Sampling Program Field Sample ID MW-31 08082022 Sampling Event August Monthly Purge Date & Time 8/8/2022 7:30 Sample Date & Time 8/8/2022 13:40 !Sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C)20 Purging Method 2 Casings Previous Well Sampled N/A Casing Volume (gal) 39.37 Calculated Casing Volumes Purge Duration (min) 362.91 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in)4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 69.70 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 8/8/2022 13:37 79.63 3438 7.40 15.60 293 2.5 114.0 8/8/2022 13:38 79.85 3433 7.38 15.40 293 2.0 114.0 8/8/2022 13:39 80.07 3436 7.36 15.43 293 1.9 114.3 8/8/2022 13:40 80.29 3437 7.35 15.44 293 1.8 114.5 Pumping Rate Calculations I Volume of water purged (gals) 80.29 Flow Rate (Q = S/60) (gal/min).217 Time to evacuate 2 Casing Volumes (min) 370.00 I Final Depth to Water (feet) 73.85 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y Sulfate y WATER 1 250-ml HOPE u None N Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals - U only y WATER 1 250-ml HOPE y HN03 (pH<2) y Comments: I Arrived on site at 0725. Purge began at 0730. Purged well for a total of 370 minutes. Purge ended and samples collected at 1340. Water was clear. Left site at 1346. Signature of Field Technician � . / //. / ___ ) __ ,..., :.r ... �_..:c_ _ _... -f-; .� --� ��1 <- Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume O Calculated Casing Volumes Purge Duration () pH Buffer 7.0 pH Buffer 4.0 Specific Conductance () Date/Time !Volume of water purged() !Final Depth to Water (feet) Gallons Purged Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Chloride Nitrate/nitrite as N Heavy Metals - U and Se only Total Dissolved Soilds Comments: I Duplicate of MW-30 Signature of Field Technician Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-65 Sampling Program MW-65_08092022 Sampling Event August Monthly 8/9/2022 10:50 !sampler TH/DL Weather Conditions External Ambient Temperature () Previous Well Sampled Well Depth (ft) Well Casing Diameter () Depth to Water Before Purging (ft) Conductivity pH Temp Redox Turbidity Dissolved Oxygen I Before/After I Pumping Rate Calculations Flow Rate {Q = S/60) () Time to evacuate 2 Casing Volumes () Number of casing Volumes Volume, if well evacuated to dryness() Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 500-ml Poly u None N y WATER 1 250-ml HDPE u H25O4 (pH<2), 4 Deg C y y WATER 1 250-ml HDPE y HNO3 (pH<2) y y WATER 1 250-ml HDPE u 4 Deg C y Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7 .0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 9/21/2022 10:27 9/21/2022 10:28 9/21/2022 10:29 9/21/2022 10:30 !Volume of water purged (gals) )Final Depth to Water (feet) 57.93 58.15 58.37 58.59 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Chloride Heavy Metals -Mn only Sulfate Nitrate/nitrite as N Total Dissolved Soilds Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-11 Sampling Program MW-11 09212022 Sampling Event September Monthly 9/21/2022 6:00 9/21/2022 10:30 !sampler TH/DL Pump Weather Conditions Cloudy with rain QED External Ambient Temperature (C)16 2 Casings Previous Well Sampled MW-26 29.20 269.14 7.0 Well Depth (ft) 130.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 85.28 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3050 7.05 15.40 421 2.1 1.2 3069 7.06 14.75 419 2.3 1.0 3051 7.05 14.70 417 2.0 1.0 3067 7.08 14.73 416 2.1 1.0 Pumping Rate Calculations 58.59 Flow Rate (Q = S/60) (gal/min).217 Time to evacuate 2 Casing Volumes (min) 270.00 87.04 Number of casing Volumes 2.00 Volume. if well evacuated to dryness {) 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 500-mL Poly u None N y WATER 1 250-ml HDPE y HN03 (pH<2) y y WATER 1 250-ml HOPE u None N y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-ml HDPE u 4 Deg C y I Arrived on site at 0555. Purge began at 0600. Purged well for a total of 270 minutes. Purge ended and samples collected at 1030. Water was clear. Signature of Field Technician Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Datefrime Gallons Purged (gal) 9/20/2022 13:42 9/20/2022 13:43 9/20/2022 13:44 9/20/2022 13:45 !Volume of water purged (gals) !Final Depth to Water (feet) 44.91 45.13 45.35 45.57 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-25 Sampling Program MW-25 09202022 Sampling Event September Monthly 9/20/2022 10:15 9/20/2022 13:45 jsampler TH/DL Pump Weather Conditions Cloudy with rain QED External Ambient Temperature (C) 20 2 Casings Previous Well Sampled MW-31 21.53 198.48 7.0 Well Depth (ft) 115.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 82.02 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3177 6.59 15.20 334 0 3.7 3172 6.60 15.18 334 0 4.0 3170 6.61 15.12 334 0 4.1 3171 6.62 15.07 334 0 4.1 Pumping Rate Calculations 45.57 Flow Rate (Q = S/60) (gal/min).217 Time to evacuate 2 Casing Volumes (min) 210.00 84.98 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number I Type Sample Filtered? Type I Added? y WATER 1 I 250-ml HOPE u 4 Deg C I y I Arrived on site at 1011. Purge began at 1015. Purged well for a total of 21 O minutes. Purge ended and samples collected at 1345. Water was clear. Left site at 1348. Signature of Field Technician Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration () pH Buffer 7 .0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time 9/20/2022 10:44 !Volume of water purged() jFinal Depth to Water (feet) Gallons Purged Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Chloride Nitrate/nitrite as N voes-Chloroform Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-26 Sampling Program MW-26 09202022 Sampling Event September Monthly 9/20/2022 10:44 9/20/2022 10:45 !sampler TH/DL Pump Weather Conditions Cloudy with rain Grundfos External Ambient Temperature (C)21 2 Casings Previous Well Sampled MW-25 25.61 7.0 Well Depth (ft) 121.33 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 82.11 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3536 6.69 16.11 373 0 28.4 Pumping Rate Calculations Flow Rate (Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes () 100.43 Number of casing Volumes Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 500-ml Poly u None N y WATER 1 250-ml HDPE u H2SO4 {pH<2), 4 Deg C y y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y I Arrived on site at 1040. Samples collected at 1045. Water was clear. Left site at 1049. Signature of Field Technician Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7 .0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 9/20/2022 9:57 9/20/2022 9:58 9/20/2022 9:59 9/20/2022 10:00 !Volume of water purged (gals) I Final Depth to Water (feet) 44.91 45.13 45.35 45.57 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Chloride Nitrate/nitrite as N Heavy Metals - U and Se only Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-30 Sampling Program MW-30 09202022 Sampling Event September Monthly 9/20/2022 6:30 9/20/2022 10:00 !sampler TH/DL Pump Weather Conditions Cloudy QED External Ambient Temperature (C)17 2 Casings Previous Well Sampled N/A 22.65 208.83 7.0 Well Depth (ft) 110.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 75.30 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 2234 6.74 14.74 416 0 52.0 2271 6.77 14.78 415 0 55.0 2250 6.80 14.82 414 0 53.9 2249 6.81 14.80 413 0 54.0 Pumping Rate Calculations 45.57 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 77.90 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 500-mL Poly u None N y WATER 1 250-mL HOPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-mL HOPE y HN03 (pH<2) y I Arrived on site at 0627. Purge began at 0630. Purged well for a total of 210 minutes. Purge ended and samples collected at 1000. Water was clear. Left site at 1008. Signature of Field Technician Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 9/20/2022 12:47 9/20/2022 12:48 9/20/2022 12:49 9/20/2022 12:50 !Volume of water purged (gals) !Final Depth to Water (feet) 79.63 79.85 80.07 80.29 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Chloride Nitrate/nitrite as N Sulfate Total Dissolved Soilds Heavy Metals - U only Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-31 Sampling Program MW-31_09202022 Sampling Event September Monthly 9/20/2022 6:40 9/20/2022 12:50 !sampler TH/DL Pump Weather Conditions Cloudy QED External Ambient Temperature (C)17 2 Casings Previous Well Sampled MW-30 39.44 363.51 7.0 Well Depth (ft) 130.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 69.60 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3407 6.44 15.33 333 0 112.0 3434 6.60 15.25 331 0 112.0 3422 6.66 15.23 331 0 111.9 3428 6.70 15.21 330 0 111.5 Pumping Rate Calculations 80.29 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 370.00 73.80 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 500-mL Poly u None N y WATER 1 250-mL HDPE u H2SO4 (pH<2), 4 Deg C y y WATER 1 250-mL HDPE u None N y WATER 1 250-mL HDPE u 4 Deg C y y WATER 1 250-ml HDPE y HNO3 (pH<2) y I Arrived on site at 0635. Purge began at 0640. Purged well for a total of 370 minutes. Purge ended and samples collected at 1250. Water was clear. Left site at 1256. Signature of Field Technician �C,J--�+-/4-�� Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume() Calculated Casing Volumes Purge Duration () pH Buffer 7.0 pH Buffer 4.0 Specific Conductance () DatefTime Gallons Purged I Volume of water purged() I Final Depth to Water (feet) Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Comments: I Duplicate of MW-25 Signature of Field Technician Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-65 Sampling Program MW-65 09202022 Sampling Event 9/20/2022 13:45 !Sampler Weather Conditions External Ambient Temperature () Previous Well Sampled Well Depth (ft) Well Casing Diameter () Depth to Water Before Purging (ft) Conductivity pH Temp Redox Pumping Rate Calculations Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () Number of casing Volumes Volume, if well evacuated to dryness() Sample Container Collected? Matrix Number I Type Sample Filtered? y WATER 1 I 250-ml HDPE u September Monthly TH/DL I Turbidity Dissolved Oxygen I Before/After I Preservative Type I Added? 4 Deg C I y Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 LABOR>\TOAIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-11_07122022 Matrix: Water Date Sampled: 7/12/22 11 :20 ( akulation, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Alkalinity -Bicarb onate (as CaC03) Alkalinity -Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese,. Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Si Iver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved Result 34.9 -5.3 31.4 l.11 277 < 1.0 0.610 54.0 0.247 2.12 1390 2520 2260 < 0.0050 < 0.0005 < 0.0005 152 < 0.0250 <0.010 < 0.0100 < 0.03 < 0.0010 55.1 0.297 < 0.00050 < 0.0100 < 0.0200 7.3 0.0093 < 0.010 440 < 0.0005 < 0.10 <0.0150 < 0.01 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.250 1.0 0.100 0.100 20.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 7/15/22 13:20@ 1.1 ·c Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030E SM 23408 SM 2320 8 SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540 C SM 2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/29122 7/29/22 7/29/22 7/19/22 7/19/22 7/26/22 7/15/22 7/15/22 7/26/22 8/1/22 7/15/22 7/29/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/19/22 7/29/22 7/29/22 7/28122 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 Lab ID: 22G1280-01 Analysis Date/Time 8/8/22 8/8/22 8/8/22 8/8/22 7/19/22 7/19/22 7/26/22 7/16/22 7/16/22 7/27/22 8/1/22 7/18/22 8/8/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/21/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 I!J!Jill} Page 3 of 40 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 Ll1BOR,\T0l!IES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-11_07122022 (cont.) Matrix: Water Date Sampled: 7/12/22 11:20 \k1al, (l"fllll.) Uranium, Dissolved 0.0026 \ olal11l-Ol"j!HIII(" ( 0111110111111- Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 7/15/22 13:20@ 1.1 °C Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Lab ID: 22G 1280-01 Analysis Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Flag(s) Page 4 of 40 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 19, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-11 07122022 587184001 Ground Water 12-JUL-22 11 :20 25-JUL-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.327 The following Analytical Methods were perfonned: MDC 0.861 ------Method Descri tion EPA 903,0 Surrogate/Tracer Recovery Test Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0IO0 DNMIO0I Units PF OF Analyst Date Time Batch Method pCi/L JXC9 08/19/22 1124 2296158 ------�Analyst Comments Result Nominal Recovery% Acceptable Limits 105 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: OF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 14 of 27 SDG: 587184 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 Lt..B0fb\TORIE5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-12_07142022 Matrix: Water Date Sampled: 7/14/22 12:40 Selenium, Dissolved Uranium, Dissolved Result 0.0292 0.0216 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L Certificate of Analysis PO#: Receipt: 7/21/22 11 :40@ 0.1 ·c Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0050 0.0003 Sampled By: Tanner Holliday EPA200.8 EPA200.8 CtF WO#: 22G1743 Preparation Date/Time 8/1/22 8/1/22 Lab ID: 22G1743-01 Analysis Date/Time 8/1/22 8/1/22 Page 3 of 36 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/1801ib\TOIIIE5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-14_07132022 Matrix: Water Date Sampled: 7/13/22 13:45 ( akulalion, Anions, Tolal Cation/Anion Balance Cations, Total TDS Ratio lnor!,!allil Alka linity -Bicarbonate (as CaCO3) Alkalinity• Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \klal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved Result 50.9 -4.1 46.9 1.14 362 < 1.0 0.112 14.5 <0.100 <0.100 2140 3720 3260 < 0.0050 < 0.0005 0.0014 438 < 0.0250 <0.010 < 0.0100 < 0.03 <0.0010 145 1.70 < 0.00050 < 0.0100 < 0.0200 10.6 < 0.0050 <0.010 297 < 0.0005 < 0.10 < 0.0150 0.01 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L No ne mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL ing/L mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL Minimum Reporting Limit 1.0 1.0 0.0500 1.0 0.100 0.100 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 O.Q3 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 7/15/22 13:20@ 1.1 ·c Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030 E SM 1030 E SM 2340 B SM 2320 B SM 2320 B EPA350.1 EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM 2540 C EPA200.8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.8 EPA 200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/29/22 7/29/22 7/29/22 7/19/22 7/19/22 7/26/22 7/15/22 7/15/22 7/26/22 8/1/22 7/15/22 7/29/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/19/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 Lab ID: 22G 1280-03 Analysis Date/Time 8/8/22 8/8/22 8/8/22 8/8/22 7/19/22 7/19/22 7/26/22 7/16/22 7/16/22 7/26/22 8/1/22 7/18/22 8/8/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/21/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 Flag(s) Page 7 of 40 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Lli.BOIUT0RIE5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-14_07132022 (cont.) Matrix: Water Date Sampled: 7/13/22 13:45 Result \h-tal, (l'lllll.) Uranium, Dissolved 0.0591 \ olal ill- ( )rl!a111r ( 11111po111ul, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofonn < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis !l..!!.J.!§ mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 PO#: Receipt: 7/15/22 13:20@ 1.1 ·c Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Lab ID: 22G1280-03 Analysis Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 flfililll Page 8 of 40 GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 19, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Contact: Lakewood, Colorado 80228 Ms. Kathy Weinel Project: White Mesa Mill GW -------Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW-14 07132022 587184003 Ground Water 13-JUL-22 13:45 25-JUL-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.246 The following Analytical Methods were performed: --------Method Description EPA 903.0 Test - MDC 0.949 Surrogate/Tracer Recovery Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0lO0 DNMIO0I Units PF DF Analyst Date Time Batch Method pCi/L JXC9 08/17/22 1446 2296158 Result Analyst Comments Nominal Recovery% Acceptable Limits 109 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 16 of 27 SDG: 587184 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 ·www.ChemtechFord.comCHEMTECH·FORD Serving the lntermountain West Since 1953 L/d3O�AT0RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-24_07202022 Matrix: Water Date Sampled: 7/20/22 8:10 ( :1kula1iom Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnor:.,:anil' Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \lctal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Mangan ese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 59.6 -3.1 56.1 1.07 < 1.0 < 1.0 0.104 46.2 0.760 0.345 2800 4200 3930 < 0.0050 0.0027 0.0086 463 < 0.0250 0.113 0.0142 <0.03 0.0023 164 7.54 < 0.00050 < 0.0100 0.0699 10.9 0.0141 <0,010 441 0.0030 <0.10 <0.0150 0.11 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.0 0.100 0.100 100 20 5 0.0050 0.0005 0.0005 2.0 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0250 0.00050 0.0100 0.0200 0.5 0.0050 0.010 5.0 0.0005 0.10 0.0150 0.01 PO#: Receipt: 7/21/22 11:40@ 0.1 °C Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030 E SM l030E SM 2340 B SM2320B SM2320 B EPA350.1 EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540 C SM 2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA 200.7 EPA200.8 EPA200.8 CtF WO#: 22G1743 Preparation Date/Time 7/29/22 7/29/22 7/29/22 7/29/22 7/21/22 7/21/22 7/26/22 7/21/22 7/21/22 7/29/22 7/22/22 7/22/22 7/29/22 8/1/22 8/1/22 8/1/22 8/11/22 8/1/22 8/1/22 8/1/22 8/3/22 8/1/22 8/3/22 8/1/22 7/22/22 8/1/22 8/1/22 8/3/22 8/1/22 8/1/22 8/11/22 8/1/22 8/3/22 8/1/22 8/1/22 Lab ID: 22G1743-07 Analysis Date/Time 8/12/22 8/12/22 8/12/22 8/12/22 7/22/22 7/22/22 7/26/22 7/22/22 7/22/22 7/29/22 7/22/22 7/22/22 8/12/22 8/1/22 8/1/22 8/1/22 8/11/22 8/1/22 8/1/22 8/1/22 8/3/22 8/1/22 8/3/22 8/1/22 7/27/22 8/1/22 8/1/22 8/3/22 8/1/22 8/1/22 8/11/22 8/1/22 8/3/22 8/1/22 8/1/22 Flag(s) Page 10 of 36 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l/,SOR,\TOPlfS Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-24_07202022 (cont.) Matrix: Water Date Sampled: 7/20/22 8:10 Result \lctal, (n111t.) Uranium, Dissolved 0.0071 \ olatilt· ( )r!!anu· ( ompouml, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 7/21/22 11 :40@ 0.1 °C Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 82600 /5030A CtF WO#: 22G1743 Preparation Date/Time 8/1/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 Lab ID: 22G1743-07 Analysis Date/Time 8/1/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 Flag(s) Page 11 of 36 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: August 24, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: ------Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-24 07282022 587833001 Ground Water 28-JUL-22 07:00 29-JUL-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 2.55 +/-0.449 The following Analytical Methods were performed: Method Descri tion EPA 903.0 S�rrogate/Tracer Recovery Test MDC 0.782 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0IO0 DNMIO0l Units PF DF Analyst Date Time Batch Method pCi/L JXC9 08/19/22 1133 2300524 ____ Analyst Com111ents Result Nominal Recovery% Acceptable Limits 107 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 11 of 13 SDG: 587833 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LM�ORI\TOl!IES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-24A_07192022 Matrix: Water Date Sampled: 7/19/22 7:00 ( all'ula1ion, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnon,!anic: Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Ammonia asN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved Result 63.6 -4.4 58.2 1.03 < 1.0 < 1.0 < 0.0500 46.7 1.13 0.275 2990 4310 4170 <0.0050 0.0048 0.0086 475 < 0.0250 0.119 0.0175 <0,03 < 0.0010 161 7.10 < 0.00050 < 0.0100 0.0590 10.7 0.0161 <0.010 482 0.0027 < 0.10 < 0.0150 0.04 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.0 0.100 0.100 100 20 5 0.0050 0.0005 0.0005 2.0 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0250 0.00050 0.0100 0.0200 0.5 0.0050 0.010 5.0 0.0005 0.10 0.0150 0.01 PO#: Receipt: 7/21/22 11 :40 @ 0.1 °C Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday .M.tl!!.fil! SM 1030 E SM 1030E SM 1030 E SM 2340 B SM2320 B SM 2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM 2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22G1743 Preparation Date/Time 7129/22 7/29/22 7/29/22 7/29122 7/21/22 7/21/22 7/26/22 7/21/22 7121/22 7/29/22 7/22122 7/22122 7129/22 8/1/22 811/22 811/22 8/11/22 8/1/22 811/22 811/22 8/3/22 811/22 8/3/22 811/22 7/22/22 8/1/22 8/1/22 8/3/22 8/1/22 8/1/22 8/11/22 8/1/22 8/3/22 811/22 8/1/22 Lab ID: 22Gl 743-06 Analysis Date/Time 8/12/22 8112122 8112122 8/12122 7/22/22 7122122 7126122 7/22/22 7/22/22 7/29/22 7/22122 7/22/22 8/12/22 8/1/22 811122 811/22 8111122 8/1/22 8/1122 8/1/22 8/3/22 811/22 813122 811/22 7/27/22 8/1/22 8/1/22 8/3/22 8/1/22 8/1/22 8/11/22 8/1/22 8/3/22 8/1122 811/22 Flag(s) Page 8 of 36 I Chemtech--Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l/180RATOAIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-24A_07192022 (cont.) Matrix: Water Date Sampled: 7/19/22 7:00 Result \lctal, ( rnnt.) Uranium, Dissolved 0.0086 \ olatik ( )rganit· ( 0111po111HI, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 7/21/22 11:40@ 0.1 °C Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A CtF WO#: 22G1743 Preparation Date/Time 8/1/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 Lab ID: 22G1743-06 Analysis Date/Time 8/1/22 7/29/22 7/29/22 7/29/22 7129122 7129122 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 Page 9 of 36 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 19, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: ---Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill G W MW-24A 07192022 587184010 Ground Water 19-JUL-22 07:00 25-JUL-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 3.56 +/-0.653 The following Analytical Methods were performed: Method DescriPtio�n __ EPA 903.0 Surrogate/Tracer Recovery Test --- ----- MDC 0.981 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0lO0 DNMIO0l Units PF DF Analyst Date Time Batch Method pCi/L JXC9 08/17/22 1447 2296158 Result Analyst C:om !11.:..:e:..:..:n=ts:;._ __ Nominal Recovery% Acceptable Limi� IOI (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 23 of 27 SDG: 587184 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l/16O�.-.,T0RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-25_07132022 Matrix: Water Date Sampled: 7/13/22 11:00 ( all-ulation, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio I llOl"l!llllil' Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 40.7 -5.8 36.3 1.10 31 I < 1.0 0.453 22.4 0.171 <0.100 1680 2830 2580 < 0,0050 < 0.0005 0.0013 311 < 0.0250 <0.010 < 0.0100 < 0.03 < 0.0010 114 1.27 < 0.00050 0.0155 < 0.0200 8.5 < 0.0050 < 0.010 256 0.0008 < 0.10 < 0.0150 <0.01 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.0 0.100 0.100 20.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 7/15/22 13:20@ 1.1 ·c Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030E SM 1030E SM 1030 E SM 2340 B SM 2320 B SM2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540 C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/29/22 7/29/22 7/29/22 7/19/22 7/19/22 7/26/22 7/15/22 7/15/22 7/26/22 8/1/22 7/15/22 7/29/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/19/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 Lab ID: 22G 1280-04 Analysis Date/Time 8/8/22 8/8/22 8/8/22 8/8/22 7/19/22 7/19/22 7/26/22 7/16/22 7/16/22 7/26/22 8/1/22 7/18/22 8/8/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/21/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 Page 9 of 40 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l/,BOfi:,\TOP.IES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-25_07132022 (cont.) Matrix: Water Date Sampled: 7/13/22 11:00 \ktals ( rnnt.) Uranium, Dissolved 0.0065 \ olat,I,· Or!!ani1· ( 0111pou111h Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofonn < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 7/15/22 13:20@ 1.1 ·c Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Lab ID: 22G 1280-04 Analysis Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 .E!.!!.wl Page 10 of 40 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: August 19, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: ---Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-25 07132022 587184004 Ground Water l 3-JUL-22 11 :00 25-JUL-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.253 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.915 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (\-sigma). RL 1.00 Project: Client ID: DNMIO0IO0 DNMIO0l Units PF OF Analyst Date Time Batch Method pCi/L JXC9 08/19/22 0830 2296158 ------'Analyst Comments __ Result Nominal Recovery% Acceptable Limits 106 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: OF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 17 of 27 SDG: 587184 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/i 60R,\TQ RI ES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-26_07142022 Matrix: Water Date Sampled: 7/14/22 8:00 ( ak11lal1111" Anions, Total Cation/Anion Balance Cations, Total TDS Ratio 11101 !_!anil Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Di ssolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved Result 42.7 6.9 49.1 1.09 315 < 1.0 0.487 61.0 0.196 1.63 1720 3140 2880 < 0.0050 < 0.0005 0.0006 434 < 0.0250 <0.010 < 0.0100 < 0.03 < 0.0010 187 0.942 < 0.00050 < 0.0100 < 0.0200 7.2 0.0077 <0.010 273 < 0.0005 <0.10 < 0.0150 < 0.01 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.0 0.100 0.100 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 7/15/22 13:20@ 1.1 ·c Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030 E SM 2340 B SM 2320B SM 2320B EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540 C SM2540 C EPA200.8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA 200.7 EPA200.8 EPA200.8 CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/29/22 7/29/22 7/29/22 7/19/22 7/19/22 7/26/22 7/19/22 7/18/22 7/26/22 7/19/22 7/15/22 7/29/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/19/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 Lab ID: 22G 1280-09 Analysis Date/Time 8/8/22 8/8/22 8/8/22 8/8/22 7/20/22 7/20/22 7/26/22 7/19/22 7/19/22 7/26/22 7/19/22 7/18/22 8/8/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/21/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 .E!filfill Page 19 of 40 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 Lld30RATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-26_07142022 (cont.) Matrix: Water Date Sampled: 7/14/22 8:00 Result \h-1al, trnnl.) Uranium, Dissolved 0.0524 \ ola11h· On.!:11111· ( 1111111111111th Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < LO Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 7/15/22 13:20@ 1.1 °C Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Lab ID: 22G 1280-09 Analysis Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Flag(s) Page 20 of 40 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: August 19, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW ---- Parameter Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW-26 07142022 587184007 Ground Water 14-JUL-22 08:00 25-JUL-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 1.67 +/-0.429 The following Analytical Methods were performed: Method Description EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.952 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0I00 DNMIO0I Units PF DF Analyst Date Time Batch Method pCi/L JXC9 08/17/22 1446 2296158 Result Analyst Comments Nominal Recovery% Acceptable Limits 105 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 20 of 27 SDG: 587184 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 CHEMTECH·FORD Serving the lntermountain West Since 1953 Ll180�ATORl£S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-27_07152022 Matrix: Water Date Sampled: 7/15/22 10:45 lnor1,!anil- 0.530 5.18 Project Name: 3rd Quarter Ground Water 2022 Certificate of Analysis PO#: Receipt: 7/21/22 11 :40@ 0.1 °C Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 0.100 0.500 Sampled By: Tanner Holliday EPA300.0 EPA353.2 CtF WO#: 22G1743 7/21/22 8/2/22 Lab ID: 7/22/22 8/2/22 Page 4 of 36 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-28_07152022 Matrix: Water Date Sampled: 7/15/22 14:35 lnorg,rnir Chloride Nitrate+ Nitrite, Total, as N \let ah Selenium, Dissolved Uranium, Dissolved 159 5.16 0.0208 0.0124 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com � mg/L mg/L mg/L mg/L Certificate of Analysis PO#: Receipt: 7/21/22 11 :40@ 0.1 ·c Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 10.0 0.500 0.0050 0.0003 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 EPA200.8 EPA200.8 CtF WO#: 22G1743 Preparation Date/Time 8/11/22 8/2/22 8/1/22 8/1/22 Lab ID: 22G1743-03 Analysis Date/Time 8/12/22 8/2/22 8/1/22 8/1/22 B.rurul Page 5 of 36 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA6O1tAT0IIIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-29_07142022 Matrix: Water Date Sampled: 7/14/22 13:20 Uranium, Dissolved 0.0151 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L Certificate of Analysis PO#: Receipt: 7/21/22 11:40@ 0.1 °C Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 Sampled By: Tanner Holliday EPA200.8 CtF WO#: 22G1743 Preparation Date/Time 8/1/22 Lab ID: 22Gl 743-04 Analysis Date/Time 8/1/22 Flag(s) Page 6 of 36 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD l/,8Of•rnT0RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-30_07132022 Matrix: Water Date Sampled: 7/13/22 10:35 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis PO#: Receipt: 7/15/22 13:20@ 1.1 °C Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday CtF WO#: 22G1280 Lab ID: Page 11 of 40 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 LABOR"TOFIIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-30_07132022 (cont.) Matrix: Water Date Sampled: 7/13/22 10:35 \It-mis (1·11111.1 Uranium, Dissolved 0.0100 \ 11la1ik Oq�a1111· < 11111p1111111h Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofom1 < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 X y lenes, total < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 7/15/22 13:20@ 1.1 °C Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Lab ID: 22G1280-05 Analysis Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Page 12 of 40 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 19, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: ---Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-30 07132022 587184005 Ground Water I 3-JUL-22 10:35 25-JUL-22 Client Parameter Qualifier Result Uncertainty MDC---Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.306 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Surrogate/Tracer Recovery_ T_e_s_t __ 0.973 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0l00 DNMIO0I Units PF DF Analyst Date Time Batch Method pCi/L JXC9 08/17/22 1446 2296158 Result Analyst Comments Nominal Recovery% Acceptable Limits 106 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 18 of 27 SDG: 587184 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA8O�,\T0 RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-31_07122022 Matrix: Water Date Sampled: 7/12/22 12:45 ( aln1larwn, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \I dab Arsenic, Dissolved Beryllium, Dissolved Cad mium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 41.3 -4.8 37.6 I.JO 186 < 1.0 0.121 421 0.442 16.9 1260 2700 2460 < 0.0050 < 0,0005 < 0.0005 350 < 0.0250 <0,010 < 0.0100 < 0,03 <0.0010 177 < 0.0100 < 0.00050 < 0.0100 < 0.0200 7.4 0.0920 <0.010 122 < 0.0005 <0.10 < 0.0150 < 0.01 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 5.0 0.100 1.00 20.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0,03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 7/15/22 13:20@ 1.1 ·c Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030E SM 1030E SM 2340 B SM 2320 B SM 2320 B EPA350. I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540C SM 2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA 245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA 200.8 EPA200.8 CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/29/22 7/29/22 7/29/22 7/19/22 7/19/22 7/26/22 8/1/22 7/15/22 7/18/22 8/1/22 7/15/22 7/29/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/19/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 Lab ID: 22G 1280-02 Analysis Date/Time 8/8/22 8/8/22 8/8/22 8/8/22 7/19/22 7/19/22 7/26/22 8/1/22 7/16/22 7/18/22 8/1/22 7/18/22 8/8/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/21/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 Flag(s) Page 5 of 40 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/180R,,TOIIIE5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-31_07122022 (cont.) Matrix: Water Date Sampled: 7/12/22 12:45 \lclal, (n111I.) Uranium, Dissolved 0.0226 \ olalik ( )ri:anu· ( 01111111111111, Acetone < 20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 7/15/22 13:20@ 1.1 °C Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Lab ID: 22G 1280-02 Analysis Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Page 6 of40 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 19, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-31 07122022 587184002 Ground Water 12-JUL-22 12:45 25-JUL-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 1.22 +/-0.412 The following Analytical Methods were performed: Method Description EPA 903.0 Surrogate/Tracer Recovery Test MDC 1.01 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0JO0 DNMIO0l Units PF DF Analyst Date Time Batch Method pCi/L JXC9 08/17/22 1446 2296158 Result Nominal Recovery% Acceptable Limits 104 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: OF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 15 of 27 SDG: 587184 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH•FORD Serving the lntermountain West Since 1953 LA60R,\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-32_07152022 Matrix: Water Date Sampled: 7/15/22 12:20 Chloride 28.2 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L Certificate of Analysis PO#: Receipt: 7/21/22 11 :40 @ 0.1 ·c Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 1.0 Sampled By: Tanner Holliday Method EPA300.0 CtF WO#: 22G1743 Preparation Date/Time 7/21/22 Lab ID: 22Gl 743-05 Analysis Date/Time 7/22/22 Flag(s) Page 7 of 36 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 L/J.80fil,\TO RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-36_07132022 Matrix: Water Date Sampled: 7/13/22 12:30 ( :tll'lilat,on, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio I 11or1!anil' Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated 1\ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved Result 65.8 -8.1 55.9 1.04 270 < 1.0 < 0.0500 45.4 0.188 0.174 2890 4380 4210 < 0.0050 < 0.0005 < 0.0005 401 < 0.0250 < 0.010 < 0.0100 <0.03 < 0.0010 133 < 0.0100 < 0.00050 < 0.0100 < 0.0200 8.7 0.233 <0.010 612 0.0006 <0.10 < 0.0150 <0.01 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.0 0.100 0.100 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 5.0 0.0005 0.10 0.0150 0.01 PO#: Receipt: 7/15/22 13:20@ 1.1 °C Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030 E SM 1030 E SM2340B SM 2320B SM 2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540 C SM2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA 200.7 EPA200.8 EPA200.8 CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/29/22 7/29/22 7/29/22 7/19/22 7/19/22 7/26/22 7/15/22 7/15/22 7/26/22 8/1/22 7/15/22 7/29/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/19/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 Lab ID: 22G 1280-06 Analysis Date/Time 8/8/22 8/8/22 8/8/22 8/8/22 7/20/22 7/20/22 7/26/22 7/16/22 7/16/22 7/26/22 8/1/22 7/18/22 8/8/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/21/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 .E!..!!ml. Page 13 of 40 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTl:CH·FORD Serving the lntermountain West Since 1953 LA6O1Q:AT0A1ES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-36_07132022 (cont.) Matrix: Water Date Sampled: 7/13/22 12:30 Result \ li·lal, ( ro111.) Uranium, Dissolved 0.0231 \ olalih-()q!:11111" ( 111111111111uh Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofonn < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone < 20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 7/15/22 13:20@ 1.1 ·c Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20,0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Lab ID: 22G1280-06 Analysis Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Flae{s\ Page 14 of 40 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 19, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: -----Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-36 07132022 587184006 Ground Water 13-JUL-22 12:30 25-JUL-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.340 The following Analytical Methods were performed: -----------Method Test MDC 0.910 Surrogate/Tracer Recovel}' Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). Project: Client ID: DNMIO0l00 DNMIO0l RL Units PF DF Analyst Date Time Batch Method--------- 1.00 pCi/L JXC9 08/17/22 1446 2296158 Result Analyst Comments Nominal Recovel2'% Acceptable Limits 105 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 19 of27 SDG: 587184 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l.40OR:1'TOl!IE5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-38_07202022 Matrix: Water Date Sampled: 7/20/22 8:30 ( ak11ht11011, Anions, Total Cati on/Anion Balance Cations, Total TDS Ratio Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaCO3) Ammonia asN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved Result 55.0 I.I 56.2 1.06 103 < 1.0 < 0.0500 44.5 0.291 14.4 2490 3910 3680 < 0.0050 < 0.0005 < 0.0005 461 < 0.0250 <0.010 < 0.0100 <0.03 < 0.0010 190 < 0.0I00 < 0.00050 < 0.0100 < 0.0200 26.6 0.156 <0.010 387 < 0.0005 < 0.10 < 0.0150 < 0.01 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.0 0.100 1.00 100 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.0IO 0.0100 0.03 0.00IO 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 7/21/22 11 :40@ 0.1 ·c Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030E SM 1030E SM 1030 E SM 2340 B SM 2320 B SM2320B EPA350.I EPA300.0 EPA300.0 EPA 353.2 EPA300.0 SM2540C SM 2540 C EPA200.8 EPA200.8 EPA 200.8 EPA 200.7 EPA200,8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA 200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22G1743 Preparation Date/Time 7/29/22 7/29/22 7/29/22 7/29/22 7/21/22 7/21/22 7/26/22 7/21/22 7/21/22 8/2/22 7/22/22 7/22/22 7/29/22 8/1/22 8/1/22 8/1/22 8/3/22 8/1/22 8/l /22 8/1/22 8/3/22 8/1/22 8/3/22 8/1/22 7/22/22 8/1/22 8/1/22 8/3/22 8/1/22 8/1/22 8/3/22 8/1/22 8/3/22 8/1/22 8/1/22 Lab ID: 22Gl743-08 Analysis Date/Time 8/12/22 8/12/22 8/12/22 8/12/22 7/21/22 7/21/22 7/26/22 7/22/22 7/22/22 8/2/22 7/22/22 7/22/22 8/12/22 8/1/22 8/1/22 8/1/22 8/3/22 8/1/22 8/1/22 8/1/22 8/3/22 8/1/22 8/3/22 8/1/22 7/27/22 8/1/22 8/1/22 8/3/22 8/1/22 8/1/22 8/3/22 8/1/22 8/3/22 8/1/22 8/1/22 .E!.!!.lilll Page 12 of 36 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 lld:IOR:•\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-38_07202022 (cont.) Matrix: Water Date Sampled: 7/20/22 8:30 \lctal, (l·onl.) Uranium, Dissolved 0.0060 \ olat11l- ( lri:ar11r ( 01111111ur1tl, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 7/21/22 11 :40@ 0.1 ·c Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22G1743 Preparation Date/Time 8/1/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 Lab ID: 22Gl 743-08 Analysis Date/Time 8/1/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 Flag/s) Page 13 of 36 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 - www.gel.com Certificate of Analysis Report Date: August 19, 2022 Company: Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW ---------MW-38 07202022 587184012 Ground Water 20-JUL-22 08:30 25-JUL-22 Client Parameter Qualifier Result Uncertainty MDC Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.304 0.928 The following Analytical Methods were performed_: __Method ___ _ Description EPA 903.0 Surrogate/Tracer Recovery Test Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). RL 1.00 Project: Client ID: DNMIO0I00 DNMIO0l Units PF DF Analyst Date Time Batch Method pCi/L JXC9 08/17/22 1447 2296158 Result Analyst Comf)!ents Nominal Recovery% Acceptable Limits 99.3 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 24 of 27 SDG: 587184 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORO Serving the lntermountain West Since 1953 ll160RATOMIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-39_07142022 Matrix: Water Date Sampled: 7/14/22 9:35 ( alr11la111111\ Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnoq,!anit· Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Ammonia asN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \Jctal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 65.4 -10 53.1 0,720 < 1.0 < 1.0 0.231 42.5 0.555 1.34 3090 2960 4130 < 0.0050 0.0059 0.0025 386 < 0.0250 0.060 0.0222 2.09 < 0.0010 183 2.33 < 0.00050 < 0.0100 0.0309 11.9 0.0068 <0.010 421 0.0039 <0.10 < 0.0150 0.19 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.0 0.l00 0.100 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0,2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0,01 PO#: Receipt: 7/15/22 13:20@ 1.1 ·c Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030E SM2340B SM 2320 B SM 2320 B EPA350.I EPA300.0 EPA 300.0 EPA353.2 EPA300.0 SM 2540 C SM 2540 C EPA200.8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.J EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/29/22 7/29/22 7/29/22 7/19/22 7/19/22 7/26/22 7/18/22 7/18/22 7/26/22 7/19/22 7/18/22 7/29/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/19/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 Lab ID: 22G 1280-07 Analysis Date/Time 8/8/22 8/8/22 8/8/22 8/8/22 7/20/22 7/20/22 7/26/22 7/18/22 7/18/22 7/26/22 7/19/22 7/18/22 8/8/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/21/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 Page 15 of 40 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORO Serving the lntermountain West Since 1953 Ll,80R,\TOAIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-39_07142022 (cont.) Matrix: Water Date Sampled: 7/14/22 9:35 Result \lt•lal, f 1•11111.) Uranium, Dissolved 0.0114 \ ulalilt· Oq!a1111· ( 11111p1111111h Acetone < 20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com nits mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 7/15/22 13:20@ 1.1 °C Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Lab ID: 22G 1280-07 Analysis Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 flag(s) Page 16 of 40 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 19, 2022 Company: Address: Contact: Project: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW------- -- -- --Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW-39 07142022 587184008 Ground Water 14-JUL-22 09:35 25-JUL-22 Client Parameter __ __Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 2.04 +/-0.475 The following Analytical Methods were performed: _ ��Method Descri_P.tion ___ _ EPA 903.0 Surrogate/Tracer Recove12'.._ Test MDC RL 0.904 1.00 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). Project: Client ID: DNMIO0J00 DNMIO0I Units PF DF Analyst Date Time Batch Method pCi/L ------- JXC9 08/17/22 1447 2296158 _ _Anal st Corrm1ents Result _1-!ominal �ecovery% Acce_e,table Limits 103 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 21 of 27 SDG: 587184 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/18ORAT0RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-40_07142022 Matrix: Water Date Sampled: 7/14/22 10:00 ( ak11la1io11, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \kral, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cabal!, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved Result 49.8 -3.5 46.4 1.13 215 < 1.0 < 0,0500 34.3 0.391 2.13 2180 3630 3220 < 0.0050 <0.0005 < 0.0005 429 < 0.0250 <0.010 < 0.0100 < 0.03 < 0.0010 149 0.130 < 0.00050 < 0.0100 < 0.0200 9.4 0.209 < 0.010 289 < 0.0005 < 0.10 < 0.0150 <0.01 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.0 0.100 0.100 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 O.D3 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0,01 PO#: Receipt: 7/15/22 13:20@ 1.1 ·c Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday Mtll!ill!. SM 1030 E SM 1030 E SM 1030 E SM 2340 B SM2320 B SM 2320 B EPA350.\ EPA300.0 EPA300.0 EPA353.2 EPA 300.0 SM 2540 C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/29/22 7/29/22 7/29/22 7/19/22 7/19/22 7/26/22 7/18/22 7/18/22 7/26/22 7/19/22 7/18/22 7/29/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/19/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/29/22 Lab ID: 22G 1280-08 Analysis Date/Time 8/8/22 8/8/22 8/8/22 8/8/22 7/20/22 7/20/22 7/26/22 7/18/22 7/18/22 7/26/22 7/19/22 7/18/22 8/8/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 7/29/22 7/28/22 7/29/22 7/28/22 7/29/22 7/21/22 7/29/22 7/29/22 7/28/22 7/29/22 7/29/22 8/1/22 7/29/22 7/28/22 7/29/22 7/29/22 f"IAg(s) Page 17 of40 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHl:MTl:CH·f'ORD Serving the lntermountain West Since 1953 LA80"1ATOAIE5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-40_07142022 (cont.) Matrix: Water Date Sampled: 7/14/22 10:00 Result Uranium, Dissolved 0.0201 \ olalih- Org:1111r I ,11111111111111, Acetone < 20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 7/15/22 13:20@ 1.1 ·c Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Mclhod EPA200.8 EPA 82600 /S0J0A EPA 82600 /SOJDA EPA 8260D /SOJDA EPA 8260D /SOJDA EPA 8260D /SOJDA EPA 82600 /S0JOA EPA 82600 /SOJDA EPA 8260D /SOJDA EPA 8260D /SOJDA EPA 82600 /S030A EPA 8260D /SOJDA CtF WO#: 22G1280 Preparation Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Lab ID: 22G 1280-08 Analysis Date/Time 7/29/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Page 18 of 40 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 19, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard ---Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-40 07142022 587184009 Ground Water 14-JUL-22 10:00 25-JUL-22 Client Parameter __ __Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.280 The following Analytical Methods were performed: Method ----- ---1 Surrogate/Tracer Recovery Test MDC 0.899 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: DNMIOO 100 Client ID: DNMIOO l Units PF DF Analyst Date Time Batch Method pCi/L Result JXC9 08/17/22 1447 2296158 Analyst Comments __ Nominal Recovery¾ 94.6 Acceptable Lim its (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 22 of 27 SDG: 587184 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L A60R ,\TO A IE S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-65_07202022 Matrix: Water Date Sampled: 7/20/22 8:30 ( ak11la1i1111, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnorgank Alkalinity• Bicarbonate (as CaCO3) Alkalinity• Carbonate (as CaCO3) Ammonia asN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 54.7 4,5 59.8 1.06 102 < 1.0 < 0.0500 44.4 0.395 14.1 2480 3950 3720 < 0.0050 < 0.0005 < 0.0005 509 < 0.0250 <0.010 <0.0100 <0.03 <0.0010 206 < 0.0100 < 0,00050 < 0.0100 < 0.0200 27.0 0.154 <0.010 386 < 0.0005 <0.10 < 0.0150 <0.01 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.0 0.100 1.00 100 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 O.Q3 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 7/21/22 11 :40@ 0.1 ·c Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday M£!.!!.2!! SM 1030E SM 1030 E SM l030E SM2340B SM2320 B SM 2320 B EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22G1743 Preparation Date/Time 7/29/22 7/29/22 7/29/22 7/29/22 7/21/22 7/21/22 7/26/22 7/21/22 7/21/22 8/2/22 7/26/22 7/22/22 7/29/22 8/1/22 8/1/22 8/1/22 8/3/22 8/1/22 8/1/22 8/1/22 8/3/22 8/1/22 8/3/22 8/1/22 7/22/22 8/1/22 8/1/22 8/3/22 8/1/22 8/1/22 8/3/22 8/1/22 8/3/22 8/1/22 8/1/22 Lab ID: 22Gl 743-09 Analysis Date/Time 8/12/22 8/12/22 8/12/22 8/12/22 7/21/22 7/21/22 7/26/22 7/22/22 7/22/22 8/2/22 7/26/22 7/22/22 8/12/22 8/1/22 8/1/22 8/1/22 8/3/22 8/1/22 8/1/22 8/1/22 8/3/22 8/1/22 8/3/22 8/1/22 7/27/22 8/1/22 8/1/22 8/3/22 8/1/22 8/1/22 8/3/22 8/1/22 8/3/22 8/1/22 8/1/22 Flag(s) Page 14 of 36 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD l.AOO•Af"O�H:S Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-65_07202022 (cont.) Matrix: Water Date Sampled: 7/20/22 8:30 Result Uranium, Dissolved 0.0060 \ olalik Oq,:a111,· ( 11111pouml, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 7/21/22 11 :40@ 0.1 °C Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22G1743 Preparation Date/Time 8/1/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 Lab ID: 22G1743-09 Analysis Date/Time 8/1/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 7/29/22 .E!.aWl Page 15 of 36 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LAOO�ATO"IES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 7/12/22 11:20 \ olal ih- ( h!!a1111· I 0111po11111I, Acetone Benzene Carbon Tetrachloride Chloroform Chloromelhane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total Result <20.0 < 1.0 < 1.0 < 1.0 < 1.0 <20.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Minimum Reporting Limit 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 PO#: Receipt: 7/15/22 13:20@ 1.1 °C Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 Sampled By: Tanner Holliday Method EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22G1280 Preparation Date/Time 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Lab ID: 22Gl280-10 Analysis Date/Time 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 7/18/22 Page 21 of 40 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FOR0 Serving the lntermountain West Since 1953 L/1&0R>\TORIE5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 7/19/22 7:00 \ olatik ( )rcanil' ( u111pu11111h Acetone Benzene Carbon Tetrachloride Chloroform Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total <20.0 < 1.0 < 1.0 < 1.0 < 1.0 <20.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 7/21/22 11 :40@ 0.1 ·c Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 Minimum Reporting Limit 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA 82600 /5030A EPA 82600 /5030A EPA 82600 15030A EPA 82600 /5030A EPA 82600 15030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22G1743 Preparation Date/Time 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 Lab ID: 22Gl 743-10 Analysis Date/Time 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 7/30/22 Page 16 of 36 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: August 19, 2022 Company: Address: Contact: Project: ---Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-65 07202022 587184013 Ground Water 20-JUL-22 08:30 25-JUL-22 Client Parameter Qualifier Result Uncertainty MDC Rad Gas Flow Proportional Counting ---- -- GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 1.14 +/-0.354 0.884 The following Analytical Methods were performed:--Method __Qescri tio_!!_ I EPA 903.0 Surrogate/Tracer Recovery Test Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 - -- -- -- ----Project: Client ID: DNMIOOIOO DNMIOOI Units PF DF Analyst Date Time Batch Method pCi/L JXC9 08/17/22 1447 2296158 _ Analyst Comments Result Nominal Recovery% Acceptable Limit� 109 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 25 of27 SDG: 587184 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit 9632 South 500 West CHEMTECH-FORD LA80f;:ATO �IE S 8/11/2022 Work Order: 22G 1280 Pro_ject: 3rd Quarter Ground Water 2022 Energy Fuels Resources, Inc. Attn: Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Client Service Contact: 801.262.7299 The analyses presented on this report were performed in accordance with the National Environmental Laboratory Accreditation Program (NELAP) unless noted in the comments, flags, or case narrative. If the report is to be used for regulatory compliance, it should be presented in its entirety, and not be altered. Approved By: �� Melissa Connolly, Project Manager Sandy, Utah 84070 801.262.7299 Main 866.792.0093 Fax Serving the lntermountain West since 1953 www.ChemtechFord.com Page 1 of 40 LABORAfOltlES Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2022 Project Manager: Tanner Holliday Laboratory ID 22G1280-01 22G1280-02 22G1280-03 22G1280-04 22G1280-05 22G1280-06 22G1280-07 22G1280-08 22G1280-09 22G1280-10 Sample Name MW-11_07122022 MW-31_07122022 MW-14_07132022 MW-25_07132022 MW-30_07132022 MW-36_ 07132022 MW-39_07142022 MW-40_07142022 MW-26_07142022 Trip Blank Work Order Report Narrative Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions There are no corrective actions associated with this work order. Project Name: 3rd Quarter Ground Water 2022 CtF WO#: 22G1280 Page 2 of 40 CHEMTECH·FORD LABOR�\TORIES Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com Certificate of Analysis Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations ND = Not detected at the corresponding Minimum Reporting Limit (MRL). PO#: Receipt: 7/15/22 13:20 @ 1.1 ·c Date Reported: 8/11/2022 Project Name: 3rd Quarter Ground Water 2022 I mg/L = one milligram per I iter or I mg/kg= one milligram per kilogram = 1 part per million. 1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion I ng/L = one nano gram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion. Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 22G1280 Page 22 of 40 2 3 4 5 6 8 9 American West Analytical Laboratories CHAIN OF CUSTODY UPS GROUND All analysis will be ooncu:ted using NELAP accn,cjted m- and ail clatl wil be repooed usir1g AWA!. 's -.iant analyte lists and TRACKING#: 1Z 187 Y4Y 03 9757 9912 --I Client _E_n_e_ru __ Fu_e_Js_Reso __ urc __ es_,_In_c_. ______________ 1 Address: _6_4_2_5_8_._H_wy_._19_1 ________________ _ Blanding, UT 84511 Contact: Tanner Holliday Phone#: _(4_3_5_)_6_7_8_-_2_22_1 ____ _ Cell#: __________ _ Email: thoJUday@:eneqJfaela.com; KWelDd'.!:eaeqyfaela.com Project Name: 3rd Quarter Ground Water 2022 Project#: --------------------------1 PO#: Sampler Name: Tanner Holliday ?-ZC:7/\2�0 Sam_JJle ID: IIW-11 07122022 IIW-31 07122022 IIW-14_07132022 IIW-25 07132022 IIW-30 07132022 MW-36_07132022 MW-39 07142022 IIW-40 07142022 IIW-26 07142022 Date Sampled 7/12/2022 7/12/2022 7/13/2022 7/13/2022 7/13/2022 7/13/2022 7/14/2022 7/14/2022 7/14/2022 Time Sampled 1120 1245 1345 1100 1035 1230 9315 1000 800 e C � 0 (.) 'o .. 7 7 7 7 7 7 7 (1 7 reporting limits (POI.) lB1less spadr,ca11y �""- on INs Chain of CUsmdy andlor - doanlemtion QC Level: I Tum Around Time: Ur4ess oiler anangemenlS have_, m-. sigred""°"" wil be em_, by 5.1l0 pm on Standard lhe<Jayllleyae<kle. X Include EDD: LOCUS UPLOAD :::; EXCEL... ... X Field Fiftered For: :x: ---:::; Dlaolwed Ketals -c vi :::; � ... ('I .t5 ,i � a. z For Compliance With: c::i ,.;c 0 NELAP r,.. N 0 RCRA c"" ('I ';1 >0 CWA c::i c::i CJ :i 0 SDWA ") iii" c:, 0 0 ELAPIA21.A ... �CJ c 0 NUAP 0 c:, rn c:;-V} c:, ('I •□ Non-Compliance ") c:, "J "ii CJ i::: � .. II) � .....,; G" D Other: 0 � •... � 0 G" 'S :a CJ < • )( c:, � c:, 0 \() s l') c:, i ... 0 "Ill ,i .; � ('I .. 0 II) II) ii •II) rn � Known Hazards � z � � .!: .. -6 -0 .,; z IQ •a. c,i l') Ill -e •<0 & E • a g .. 0 = ;;" � • i5 ,g Sample Comments fl) z z 0 w X X X X X X X X X X w X X X X X X X X X X w X X X X X X X X X X w X X X X X X X X X X w X X X X X X X X X X w X X X X X X X X X X w X X X X X X X X X X w X X X X X X X X X X w X X X X X X X X X X AWAL lab Sample Set# Page of I'""""" Laboratory Use Only !Samples Were: 1 Slil>Pedorhanl- 2 Ambienlorc:Mled _lJ_ Temperaue t ' "C 4 R-..,., Bmkenll.eal;lng (Im�-> y 5 Propaty-y N Ched<80 at -y N 6 R---�rmes y N ICOC Tape Was: �onOl&Pacllage y N NA 2 -....on 0...-Package N NA 3 Preser1I on 5anple y N NA 4 U-..:.mSample N NA Between Sample o Trip Blank 7/12/2022 1120 � andCOC Rea,,.r? 3 w X y N Special Instructions: (/ 111mc. f''•v\ ,/\ 1',-y, T:;::> n. I'"'"" \'-,, •-• ') 0 ll"""'�,::Nam�e:�---�T:::anner:.::Ho11:::•:::;i-:,_ __ .;;.. _______ -.:�---.:.1,:::1"�-�N�IWll�. �"'�..a;�;;;.;:....:;:--"·L..:. 11..._ \��.,;;:;., .... r-:>,._.• r1.·1.'..:'1'"1"",\--'-➔=-1...., -'.....,__v-__ 11Sample containers for metals were field filtered. See the :"""by. 0-=::':by: P-Analytical Scope of Work for Reporting Limits and VOC analyte ���--------------------1::1,,=.,.,,-----F:li:.::=-----------------f;IT":;:•me;;;:--, -----111ist. Print- lsianatu-e """'Name: l<elinquioho<I by. ISlana11n ll'r1t11Name; 1••u<r I031G: rr■no: P11n1Name- flffne: PrlnlName: iuate: Tme: IPnnt Name: Page 23 of40 I Work Order# __ 2_2_y_.__l 2.._W=-" _ Delivery Method: a11PS d D Fe Ex D Walk-in Sample• t -Cf D USPS h D C emtech Courier o Customer Courier ! Chemtech Lot. Container Preservative IJn 11 'Jff 17' /./,M llPC Yz... P ,.,,, . 1� I w 11-011�: � t s . j ... i l iE Ii !! 0 "' � s. 'll J 1.! i I � i Misc l Volume l! 107/llllJ ;;: CHEMTECH FORD LABORATORIES Sample Receipt Receiving Temperature l, I oc -•' -· Comments CHEMTECH-FORD LABORATOi!ltS Sample Condition (checklf)eS) IR"custody Seals P'tontainers Intact !(°coc can be matched to bottles lit'Received on tee � Correct Containers(s) �rficent Sample Volume 0 Headspace Present (VOC) �mperature Blank �ceived within Holding Time Plastic Containers A· Pl.utlc Un-rvi,d 8-Miscellaneous Plastic C-Cyanide Qt (Na0H) E• Colifonn/Ecoli/HPC F-Sulfide Qt (Zn Acetate) l• Mercury 1631 M• M<'tals Pint {HN03) N-Nutrient Pint (H2S04) R· Radiological {HN03) S• Sludge Cups/Tubs Q· Plastic Bag Glass Contain�rs D- 625 {Na25203) G-Glass Unpreserved H-HAAs {NH4CI) J· 508/515/525 (Na2503) l<-515.3 Herbicides 0-Oil & Grease {HCI) P-Phenols (H2S04) T-T0C/T0X (H3P04) U· 531 (MCAA, Na2S203) V-524/THMs {Ascorbic Acid) W- 8260 voe {1:1 HCI) X.· Vial Unpreserved V· 624/504 {Na2S203) Z- Miscellaneous Glass Page 24 of 40 QC Report for Work Order (WO) -22G1280 Analyte % Rec RPO Limits RPO Max Result Source Cone SpkValue MRL DF Blank -EPA 200.7 QC Sample ID: BWG1311-BLK1 Batch: BWG1311 Date Prepared: 07/28/2022 Date Analyzed: 07/28/2022 Calcium, Dissolved ND 0.2 1.00 Iron, Dissolved ND 0.03 1.00 Magnesium, Dissolved ND 0.2 1.00 Potassium, Dissolved ND 0.5 1.00 Sodium, Dissolved ND 0.5 1.00 Tin, Dissolved ND 0.10 1.00 LCS -EPA 200. 7 QC Sample ID: BWG 13 l l-BS I Batch: BWG131 I Date Prepared: 07/28/2022 Date Analyzed: 07/28/2022 Calcium, Dissolved 95.8 85 -115 9.8 10.2 0.2 1.00 Iron, Dissolved 95.0 85 -115 0.190 0.200 0.02 1.00 Magnesium, Dissolved 100 85 -115 10.2 10.2 0.2 1.00 Potassium, Dissolved 98.3 85 -115 9.8 10.0 0.5 1.00 Sodium, Dissolved 98.2 85 -115 9.8 10.0 0.5 1.00 Tin, Dissolved 96.9 85 -155 0.19 0.200 0.02 1.00 Matrix Spike -EPA 200.7 QC Sample ID: BWGI311-MS2 Batch: BWGI3ll QC Source Sample: 22G 1280-0 I Date Prepared: 07/28/2022 Date Analyzed: 07/28/2022 Calcium, Dissolved 139 70 -130 166 152 10.2 0.2 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Iron, Dissolved 91.5 70 -130 0.183 ND 0.200 0.02 1.00 Magnesium, Dissolved 106 70 -130 65.9 55.1 10.2 0.2 1.00 Potassium, Dissolved 88.4 70 -130 16.2 7 .3 10.0 0.5 1.00 Sodium.Dissolved -113 70-130 428 440 10.0 0.5 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to arialyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Tin, Dissolved 80.5 70 -130 0.16 Matrix Spike Dup -EPA 200.7 QC Sample ID: BWG1311-MSD2 Batch: BWGl31 l QC Source Sample: 22Gl280-0l Date Prepared: 07/28/2022 Date Analyzed: 07/28/2022 ND 0.200 0.02 1.00 Calcium.Dissolved 151 0.730 70-130 20 167 152 10.2 0.2 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Iron, Dissolved 91.2 0.328 70 -130 20 0.182 ND 0.200 0.02 Magnesium, Dissolved 110 0.620 70 -130 20 66.3 55.1 10.2 0.2 Potassium, Dissolved 88.7 0.180 70 -130 20 16.2 7.3 10.0 0.5 Sodium, Dissolved -119 0.146 70 -130 20 428 440 10.0 0.5 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Tin, Dissolved 82.6 2.58 70 -130 20 0.17 ND 0.200 0.02 1.00 1.00 1.00 1.00 1.00 CtF WO#: 22G1280 www.ChemtechFord.com Page 25 of 40 QC Report for Work Order (WO) -22G1280 Analyte %Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -EPA 200.8 QC Sample JD: BWGl406-BLK1 Batch: BWG1406 Date Prepared: 07/29/2022 Date Analyzed: 07/29/2022 Arsenic, Dissolved ND 0.0050 1.00 Beryllium, Dissolved ND 0.0005 1.00 Cadmium, Dissolved ND 0.0005 1.00 Chromium, Dissolved ND 0.0250 1.00 Cobalt, Dissolved ND 0.010 1.00 Copper, Dissolved ND 0.0100 1.00 Lead, Dissolved ND 0.0010 1.00 Manganese, Dissolved ND 0.0100 1.00 Molybdenum, Dissolved ND 0.0100 1.00 Nickel, Dissolved ND 0.0200 1.00 Selenium, Dissolved ND 0.0050 1.00 Silver, Dissolved ND 0.010 1.00 Thallium, Dissolved ND 0.0005 1.00 Uranium, Dissolved ND 0.0003 1.00 Vanadium, Dissolved ND 0.0150 1.00 Zinc, Dissolved ND 0.01 1.00 LCS -EPA 200.8 QC Sample ID: BWG1406-BS1 Batch: BWG1406 Date Prepared: 07/29/2022 Date Analyzed: 07/29/2022 Arsenic, Dissolved 99.5 85-115 0.040 0.0400 0.0005 1.00 Beryllium, Dissolved 112 85 -115 0.045 0.0400 0.0005 1.00 Cadmium, Dissolved 102 85 -115 0.041 0.0400 0.0002 1.00 Chromium, Dissolved 103 85 -115 0.041 0.0400 0.0005 1.00 Cobalt, Dissolved 102 85-115 0.041 0.0400 0.0005 1.00 Copper, Dissolved 99.6 85 -115 0.040 0.0400 0.0010 1.00 Lead, Dissolved 101 85 -115 0.041 0.0400 0.0005 1.00 Manganese, Dissolved 103 85-115 0.041 0.0400 0.0005 1.00 Molybdenum, Dissolved 104 85 -115 0.041 0.0400 0.0005 1.00 Nickel, Dissolved 102 85 -115 0.0410 0.0400 0.0005 1.00 Selenium, Dissolved 106 85 -115 0.042 0.0400 0.0005 1.00 Silver, Dissolved 96.9 85 -115 0.039 0.0400 0.0005 1.00 Thallium, Dissolved 104 85 -115 0.041 0.0400 0.0002 1.00 Uranium, Dissolved 102 85 -115 0.041 0.0400 0.0003 1.00 Vanadium, Dissolved 101 85-115 0.040 0.0400 0.0005 1.00 Zinc, Dissolved 105 85-115 0.04 0.0400 0.01 1.00 Matrix Spike -EPA 200.8 QC Sample ID: BWG1406-MSI Batch: BWG1406 QC Source Sample: 22G 1280-0 l Date Prepared: 07/29/2022 Date Analyzed: 07/29/2022 Arsenic, Dissolved 102 70 -130 0.041 ND 0.0400 0.0005 1.00 Beryllium, Dissolved 104 70 -130 0.042 ND 0.0400 0.0005 1.00 Cadmium, Dissolved 98.1 70 -130 0.039 0.0002 0.0400 0.0002 1.00 Chromium, Dissolved 89.1 70 -130 0.038 0.003 0.0400 0.0005 1.00 Cobalt, Dissolved 92.7 70-130 0.038 0.001 0.0400 0.0005 1.00 Copper, Dissolved 91.0 70 -130 0.037 0.0009 0.0400 0.0010 1.00 Lead, Dissolved 100 70 -130 0.040 0.00004 0.0400 0.0005 1.00 Manganese, Dissolved 100 70-130 0.337 0.297 0.0400 0.0005 1.00 Molybdenum, Dissolved 104 70 -130 0.044 0.002 0.0400 0.0005 1.00 Nickel, Dissolved 90.5 75 -125 0.0385 0.0024 0.0400 0.0005 1.00 Selenium, Dissolved 102 70 -130 0.050 0.009 0.0400 0.0005 1.00 Silver, Dissolved 71.5 70 -130 0.029 ND 0.0400 0.0005 1.00 CtF WO#: 22G1280 www.ChemtechFord.com Page 26 of 40 Analyte QC Sample JD: BWG1406-MS1 Date Prepared: 07/29/2022 Thallium, Dissolved Uranium, Dissolved Vanadium, Dissolved Zinc, Dissolved CtF WO#: 22G1280 www.ChemtechFord.com QC Report for Work Order (WO) -22G1280 %Rec RPO Limits RPO Max Result Source Cone Matrix Spike - EPA 200.8 (cont.) Batch: BWG1406 QC Source Sample: 22Gl280-0l Date Analyzed: 07/29/2022 102 70 -130 0.041 0.0003 104 70 -130 0.044 0.003 92.0 70 -130 0.037 0.0007 94.7 70 -130 0.04 0.002 Spk Value MRL OF 0.0400 0.0002 1.00 0.0400 0.0003 1.00 0.0400 0.0005 1.00 0.0400 0.01 1.00 Page 27 of40 Analyte QC Sample ID: BWG0807-BLKl Date Prepared: 07/18/2022 Mercury, Dissolved QC Sample ID: BWG0807-BSI Date Prepared: 07/18/2022 Mercury, Dissolved QC Sample ID: BWG0807-MS1 Date Prepared: 07/18/2022 Mercury, Dissolved QC Sample ID: BWG0807-MSDI Date Prepared: 07/18/2022 Me�cury, Dissolved CtF WO#: 22G1280 www.ChemtechFord.com QC Report for Work Order (WO) -22G1280 %Rec RPO Limits RPO Max Result Source Cone Blank -EPA 245.1 Batch: BWG0807 Date Analyzed: 07 /2 l /2022 ND LCS -EPA 245.1 Batch: BWG0807 Date Analyzed: 07/21/2022 97.0 85-115 0.00485 Matrix Spike -EPA 245.1 Batch: BWG0807 QC Source Sample: 22G 1280-0 I Date Analyzed: 07/21/2022 101 75 -125 0.00507 ND Matrix Spike Dup -EPA 245.1 Batch: BWG0807 QC Source Sample: 2201280-01 Date Analyzed: 07 /2 l /2022 96.9 4.68 75 -125 20 0.00484 ND Spk Value MRL OF ).0005( 1.00 0.00500 l0001E 1.00 0.00500 l0001E 1.00 0.00500 l0001E 1.00 Page 28 of 40 QC Report for Work Order (WO) -22G1280 Analyte % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL DF Blank -EPA 300.0 QC Sample ID: BWG0728-BLK1 Batch: BWG0728 Date Prepared: 07 / I 5/2022 Date Analyzed: 07/15/2022 Chloride ND 1.0 1.00 Fluoride ND 0.100 1.00 QC Sample ID: BWG0813-BLKI Batch: BWG0813 Date Prepared: 07/18/2022 Date Analyzed: 07/18/2022 Chloride ND 1.0 1.00 Fluoride ND 0.100 1.00 QC Sample ID: BWG0817-BLK1 Batch: BWG0817 Date Prepared: 07/18/2022 Date Analyzed: 07/18/2022 Chloride ND 1.0 1.00 Fluoride ND 0.100 1.00 QC Sample ID: BWG0861-BLK1 Batch: BWG0861 Date Prepared: 07/19/2022 Date Analyzed: 07/19/2022 Sulfate ND 1.0 1.00 QC Sample ID: BWH0292-BLK1 Batch: BWH0292 Date Prepared: 08/0 I /2022 Date Analyzed: 08/01/2022 Chloride ND 1.0 1.00 Sulfate ND 1.0 1.00 LCS -EPA 300.0 QC Sample ID: BWG0728-BS1 Batch: BWG0728 Date Prepared: 07/15/2022 Date Analyzed: 07/15/2022 Chloride 103 90 -110 51.4 50.0 1.0 1.00 Fluoride 95.1 90 -110 4.75 5.00 0.100 1.00 QC Sample ID: BWG0813-BS1 Batch: BWG0813 Date Prepared: 07/18/2022 Date Analyzed: 07/18/2022 Chloride 101 90 -110 50.3 50.0 1.0 1.00 Fluoride 96.4 90 -110 4.82 5.00 0.100 1.00 QC Sample ID: BWG0817-BSl Batch: BWG0817 Date Prepared: 07/18/2022 Date Analyzed: 07/18/2022 Chloride 103 90 -110 51.5 50.0 1.0 1.00 Fluoride 94.8 90 -110 4.74 5.00 0.100 1.00 QC Sample ID: BWG0861-BS1 Batch: BWG0861 Date Prepared: 07/19/2022 Date Analyzed: 07/19/2022 Sulfate 97.2 90 -110 48.6 50.0 1.0 1.00 QC Sample ID: BWH0292-BS1 Batch: BWH0292 Date Prepared: 08/01/2022 Date Analyzed: 08/01/2022 Chloride 104 90 -110 52.1 50.0 1.0 1.00 Sulfate 99.8 90 -110 49.9 50.0 1.0 1.00 Matrix Spike -EPA 300.0 QC Sample ID: BWG0728-MS2 Batch: BWG0728 QC Source Sample: 22G 1280-0 I Date Prepared: 07/16/2022 Date Analyzed: 07/16/2022 Chloride 97.2 80 -120 248 54.0 200 22.0 1.00 Fluoride 99.9 80 -120 20.0 ND 20.0 2.20 1.00 QC Sample ID: BWH0292-MS I Batch: BWH0292 QC Source Sample: 2201280-01 Date Prepared: 08/01/2022 Date Analyzed: 08/01/2022 Chloride 104 80 -120 264 55.8 200 22.0 1.00 CtF WO#: 22G1280 www.ChemtechFord.com Page 29 of 40 QC Report for Work Order (WO) -22G1280 Analyte %Rec RPO Limits RPO Max Result Source Cone Spk Value Matrix Spike - EPA 300.0 (cont.) QC Sample ID: BWH0292-MS 1 Batch: BWH0292 QC Source Sample: 22Gl280-01 Date Prepared: 08/01/2022 Date Analyzed: 08/01/2022 Sulfate 109 80 -120 1600 1390 200 Matrix Spike Dup - EPA 300.0 QC Sample ID: BWG0728-MSD2 Batch: BWG0728 QC Source Sample: 2201280-01 Date Prepared: 07/16/2022 Date Analyzed: 07/16/2022 Chloride 98.1 0.725 80-120 20 250 54.0 200 Fluoride 98.7 1.21 80 -120 20 19.7 ND 20.0 QC Sample ID: BWH0292-MSD1 Batch: BWH0292 QC Source Sample: 22G 1280-01 Date Prepared: 08/01/2022 Date Analyzed: 08/01/2022 Chloride 107 1.79 80 -120 20 269 55.8 200 Sulfate 128 2.37 80 -120 20 1640 1390 200 QM-12 -The MSD recovery was outside acceptance limits, but passed duplicate spike acceptance criteria. The batch was accepted based on the acceptability of the MS. CtF WO#: 22G1280 www.ChemtechFord.com MRL OF 22.0 1.00 22.0 1.00 2.20 1.00 22.0 1.00 22.0 1.00 Page 30 of 40 Analyte QC Sample ID: BWG1206-BLK1 Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWG1206-BS1 Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWG1206-MS1 Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWG1206-MS2 Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWG 1206-MS3 Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWG1206-MSD1 Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWG l206-MSD2 Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWG1206-MSD3 Date Prepared: 07/26/2022 Ammonia as N CtF WO#: 22G1280 www.ChemtechFord.com QC Report for Work Order (WO) -22G1280 %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 350.1 Batch: BWG1206 Date Analyzed: 07/26/2022 ND 0.0500 1.00 LCS -EPA 350.1 Batch: BWG 1206 Date Analyzed: 07/26/2022 96.2 90-110 0.962 1.00 0.0500 1.00 Matrix Spike -EPA 350.1 Batch: BWG1206 QC Source Sample: 2201280-01 Date Analyzed: 07/26/2022 87.0 80 -120 1.48 0.610 1.00 0.250 5.00 Batch: BWG1206 QC Source Sample: XXXXXXX-XX Date Analyzed: 07/26/2022 95.2 80 -120 1.06 0.104 1.00 0.0500 1.00 Batch: BWG 1206 QC Source Sample: XXXXXXX-XX Date Analyzed: 07/26/2022 98.9 80 -120 0.989 ND 1.00 0.0500 1.00 Matrix Spike Dup -EPA 350.1 Batch: BWG1206 QC Source Sample: 2201280-01 Date Analyzed: 07/26/2022 82.3 3.25 80 -120 20 1.43 0.610 1.00 0.250 5.00 Batch: BWG1206 QC Source Sample: XXXXXXX-XX Date Analyzed: 07/26/2022 97.8 2.42 80 -120 20 1.08 0.104 1.00 0.0500 1.00 Batch: BWG1206 QC Source Sample: XXXXXXX-XX Date Analyzed: 07/26/2022 103 3.55 80 - 120 20 1.03 ND 1.00 0.0500 1.00 Page 31 of40 QC Report for Work Order (WO) -22G1280 Analyte % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -EPA 353.2 QC Sample ID: BWG0770-BLK1 Batch: BWG0770 Date Prepared: 07/18/2022 Date Analyzed: 07/18/2022 Nitrate+ Nitrite, Total, as N ND 0.100 1.00 QC Sample ID: BWG1165-BLK1 Batch: BWG1165 Date Prepared: 07/26/2022 Date Analyzed: 07/26/2022 Nitrate+ Nitrite, Total, as N ND 0.100 1.00 QC Sample ID: BWGl 177-BLKl Batch: BWGll 77 Date Prepared: 07/26/2022 Date Analyzed: 07/26/2022 Nitrate+ Nitrite, Total, as N ND 0.100 1.00 LCS -EPA 353.2 QC Sample ID: BWG0770-BS1 Batch: BWG0770 Date Prepared: 07/18/2022 Date Analyzed: 07/18/2022 Nitrate + Nitrite, Total, as N 106 80 -120 2.12 2.00 0.100 1.00 QC Sample ID: BWGl 165-BSl Batch: BWG1165 Date Prepared: 07/26/2022 Date Analyzed: 07/26/2022 Nitrate + Nitrite, Total, as N 108 80 -120 2.16 2.00 0.100 1.00 QC Sample ID: BWG1177-BS1 Batch: BWG 1177 Date Prepared: 07/26/2022 Date Analyzed: 07/26/2022 Nitrate+ Nitrite, Total, as N 108 80 -120 2.15 2.00 0.100 1.00 Matrix Spike - EPA 353.2 QC Sample ID: BWG0770-MSI Batch: BWG0770 QC Source Sample: XXXXXXX-XX Date Prepared: 07/18/2022 Date Analyzed: 07/18/2022 Nitrate + Nitrite, Total, as N 96.2 80 -120 1.01 0.0460 1.00 0.100 1.00 QC Sample ID: BWG0770-MS2 Batch: BWG0770 QC Source Sample: XXXXXXX-XX Date Prepared: 07/18/2022 Date Analyzed: 07 I 18/2022 Nitrate + Nitrite, Total, as N 99.1 80 -120 1.02 0.0340 1.00 0.100 1.00 QC Sample ID: BWG1165-MS1 Batch: BWG1165 QC Source Sample: XXXXXXX-XX Date Prepared: 07/26/2022 Date Analyzed: 07/27/2022 Nitrate+ Nitrite, Total, as N 102 80 -120 1.27 0.251 1.00 0.100 1.00 QC Sample ID: BWG1165-MS2 Batch: BWG1165 QC Source Sample: 22Gl280-0l Date Prepared: 07/26/2022 Date Analyzed: 07/27/2022 Nitrate + Nitrite, Total, as N 99.7 80 -120 3.11 2.12 1.00 0.100 1.00 QC Sample ID: BWG1177-MS1 Batch: BWGI 177 QC Source Sample: XXXXXXX-XX Date Prepared: 07/26/2022 Date Analyzed: 07/27/2022 Nitrate+ Nitrite, Total, as N 97.4 80 -120 1.07 0.100 1.00 0.100 1.00 QC Sample ID: BWG1177-MS2 Batch: BWG 1177 QC Source Sample: XXXXXXX-XX Date Prepared: 07/26/2022 Date Analyzed: 07/27/2022 Nitrate+ Nitrite, Total, as N 112 80 -120 9.22 8.10 1.00 0.500 5.00 Matrix Spike Dup -EPA 353.2 QC Sample ID: BWG0770-MSD1 Batch: BWG0770 QC Source Sample: XXXXXXX-XX Date Prepared: 07/18/2022 Date Analyzed: 07 I 18/2022 Nitrate+ Nitrite, Total, as N 98.2 1.96 80 -120 20 1.03 0.0460 1.00 0.100 1.00 QC Sample ID: BWG0770-MSD2 Batch: BWG0770 QC Source Sample: XXXXXXX-XX Date Prepared: 07/18/2022 Date Analyzed: 07/18/2022 Nitrate+ Nitrite, Total, as N 100 1.26 80 -120 20 1.04 0.0340 1.00 0.100 1.00 CtF WO#: 22G1280 www.ChemtechFord.com Page 32 of 40 Nitrate+ Nitrite, Total, as N Nitrate+ Nitrite, Total, as N Nitrate + Nitrite, Total, as N Nitrate + Nitrite, Total, as N CtF WO#: 22G1280 QC Report for Work Order (WO) -22G1280 Matrix Spike Dup -EPA 353.2 (cont.) 104 1.80 80 -120 20 1.29 0.251 104 1.31 80 -120 20 3.16 2.12 96.3 1.03 80 -120 20 1.06 0.100 119 0.789 80 -120 20 9.29 8.10 1.00 0.100 1.00 1.00 0.100 1.00 1.00 0.100 1.00 1.00 0.500 5.00 Page 33 of 40 QC Report for Work Order (WO) -22G1280 Analyte QC Sample ID: BWG0844-BLK1 Date Prepared: 07/18/2022 Acetone Benzene Carbon Tetrachloride Chloroform Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total QC Sample ID: BWG0844-BS1 % Rec RPO Limits RPO Max Blank -EPA 8260D /5030A Batch: BWG0844 Date Analyzed: 07 I 18/2022 LCS -EPA 8260D /5030A Batch: BWG0844 Date Prepared: 07/18/2022 Date Analyzed: 07/18/2022 Result ND ND ND ND ND ND ND ND ND ND ND Source Cone Spk Value MRL OF 20.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 20.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 Acetone 141 70-130 141 100 10.0 1.00 HB -Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore accepted and reported for this parameter. Benzene 112 70-130 11.2 10.0 1.0 1.00 Carbon Tetrachloride 103 70 -130 10.3 10.0 1.0 1.00 Chloroform 126 70 -130 12.6 10.0 1.0 1.00 Chloromethane 150 70-130 15.0 10.0 1.0 1.00 HB -Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore accepted and reported for this parameter. Methyl Ethyl Ketone 100 70 -130 100 100 10.0 1.00 Methylene Chloride 117 70 -130 11.7 10.0 1.0 1.00 Naphthalene 103 70 -130 10.3 10.0 1.0 1.00 Tetrahydrofuran 110 70 -130 11.0 10.0 1.0 1.00 Toluene 107 70 -130 10.7 10.0 1.0 1.00 Xylenes, total 113 70 -130 33.8 30.0 1.0 1.00 Matrix Spike -EPA 82600 /5030A QC Sample ID: BWG0844-MS1 Batch: BWG0844 QC Source Sample: 2201280-01 Date Prepared: 07/18/2022 Date Analyzed: 07/18/2022 Acetone 122 70 -130 122 ND 100 10.0 1.00 Benzene 93.8 70 -130 9.38 ND 10.0 1.0 1.00 Carbon Tetrachloride 78.4 70 -130 7.84 ND 10.0 1.0 1.00 Chloroform 106 70 -130 10.6 ND 10.0 1.0 1.00 Chloromethane 149 70 -130 14.9 ND 10.0 1.0 1.00 MS-High -Estimated high due to Matrix Spike recovery. Methyl Ethyl Ketone 83.6 70-130 83.6 ND 100 10.0 1.00 Methylene Chloride 102 70 -130 10.2 ND 10.0 1.0 1.00 Naphthalene 75.3 70 -130 7.53 ND 10.0 1.0 1.00 Tetrahydrofuran 103 70 -130 10.3 ND 10.0 1.0 1.00 Toluene 90.1 70-130 9.01 ND 10.0 1.0 1.00 Xylenes, total 90.8 70-130 27.2 ND 30.0 1.0 1.00 Matrix Spike Dup -EPA 8260D /5030A QC Sample ID: BWG0844-MSD1 Batch: BWG0844 QC Source Sample: 2201280-01 Date Prepared: 07/18/2022 Date Analyzed: 07/18/2022 Acetone 121 0.840 70-130 20 121 ND 100 10.0 1.00 Benzene 92.2 1.72 70 -130 20 9.22 ND 10.0 1.0 1.00 CtF WO#: 22G1280 www.ChemtechFord.com Page 34 of 40 QC Report for Work Order (WO) -22G1280 Analyte % Rec RPO Limits RPO Max Result Source Cone Matrix Spike Dup -EPA 8260D /5030A (cont.) QC Sample ID: BWG0844-MSD1 Batch: BWG0844 QC Source Sample: 2201280-01 Date Prepared: 07/18/2022 Date Analyzed: 07/18/2022 Carbon Tetrachloride 77.0 1.80 70 -130 20 7.70 ND Chloroform 108 1.50 70 -130 20 10.8 ND Chloromethane 145 3.06 70 -130 20 14.5 ND MS-High -Estimated high due to Matrix Spike recovery. Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total CtF WO#: 22G1280 www.ChemtechFord.com 83.9 100 83.3 107 87.7 91.3 0.406 70 -130 20 83.9 ND 1.39 70-130 20 10.0 ND 10.1 70 -130 20 8.33 ND 3.14 70 -130 20 10.7 ND 2.70 70-130 20 8.77 ND 0.549 70 -130 20 27.4 ND SpkValue MRL OF 10.0 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 100 10.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 30.0 1.0 1.00 Page 35 of40 QC Report for Work Order (WO) -22G1280 Analyte % Rec RPD Limits RPD Max Result Source Cone Spk Value Blank -SM 2320 B QC Sample ID: BWG0881-BLKI Batch: BWG0881 Date Prepared: 07/19/2022 Date Analyzed: 07/19/2022 Alkalinity -Bicarbonate (as CaCO3) ND Alkalinity -Carbonate (as CaCO3) ND QC Sample ID: BWG0913-BLKI Batch: BWG0913 Date Prepared: 07/19/2022 Date Analyzed: 07/20/2022 Alkalinity -Bicarbonate (as CaCO3) ND Alkalinity -Carbonate (as CaCO3) ND Duplicate -SM 2320 B QC Sample ID: BWG0881-DUPI Batch: BWG0881 QC Source Sample: XXXXXXX-XX Date Prepared: 07/19/2022 Date Analyzed: 07/19/2022 Alkalinity -Bicarbonate (as CaCO3) 0.147 20 204 204 Alkalinity -Carbonate (as CaCO3) 20 ND ND Alkalinity -Total (as CaCO3) 0.147 20 204 204 QC Sample ID: BWG0881-DUP2 Batch: BWG0881 QC Source Sample: 22Gl280-0l Date Prepared: 07/19/2022 Date Analyzed: 07/19/2022 Alkalinity -Bicarbonate (as CaCO3) 0.144 20 277 277 Alkalinity -Carbonate (as CaCO3) 20 ND ND Alkalinity -Total (as CaCO3) 0.144 20 277 277 QC Sample ID: BWG0881-DUP3 Batch: BWG0881 QC Source Sample: XXXXXXX-XX Date Prepared: 07/19/2022 Date Analyzed: 07/19/2022 Alkalinity - Bicarbonate (as CaCO3) 0.173 20 232 231 Alkalinity -Carbonate (as CaCO3) 20 ND ND Alkalinity -Total (as CaCO3) 0.173 20 232 231 QC Sample ID: BWG0881-DUP4 Batch: BWG0881 QC Source Sample: XXXXXXX-XX Date Prepared: 07/19/2022 Date Analyzed: 07/19/2022 Alkalinity -Bicarbonate (as CaCO3) 0.0461 20 434 433 Alkalinity -Carbonate (as CaCO3) 20 ND ND Alkalinity -Total (as CaCO3) 0.0461 20 434 433 QC Sample ID: BWG0881-DUP5 Batch: BWG0881 QC Source Sample: XXXXXXX-XX Date Prepared: 07/19/2022 Date Analyzed: 07/19/2022 Alkalinity -Bicarbonate (as CaCO3) 2.12 20 424 433 Alkalinity -Carbonate (as CaCO3) 162 20 11.3 1.2 QM-020 -The RPO and/or percent recovery for this QC spike sample cannot be accurately calculated due to the low concentration of analyte inherent in the sample. The batch was accepted based on acceptable LCS recovery. Alkalinity -Total (as CaCO3) QC Sample ID: BWG0913-DUPl Date Prepared: 07/19/2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Alkalinity -Total (as CaCO3) QC Sample ID: BWG0881-BS1 Date Prepared: 07/19/2022 Alkalinity -Total (as CaCO3) QC Sample ID: BWG0913-BS1 Date Prepared: 07/19/2022 Alkalinity - Total (as CaCO3) CtF WO#: 22G1280 www.ChemtechFord.com 0.230 20 435 434 Batch: BWG0913 QC Source Sample: XXXXXXX-XX Date Analyzed: 07/20/2022 0.169 20 473 474 20 ND ND 0.169 20 473 474 LCS -SM 2320 B Batch: BWG0881 Date Analyzed: 07/19/2022 94.5 90 -110 223 Batch: BWG0913 Date Analyzed: 07/20/2022 94.7 90 - 110 224 236 236 MRL DF 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 Page 36 of 40 CtF WO#: 22G1280 QC Report for Work Order (WO) -22G1280 872 872 2 Page 37 of40 Surrogates Report for Work Order (WO) -22G1280 QCID Analyte BWG0844-BLK1 1,2-Dichloroethane-d4 BWG0844-BLK 1 4-Bromofluorobenzene BWG0844-BLK1 Toluene-dB BWG0844-BS1 1,2-Dichloroethane-d4 BWG0844-BS1 4-Bromofluorobenzene BWG0844-8S1 Toluene-dB BWG0844-MS1 1,2-Dichloroethane-d4 BWG0844-MS1 4-Bromofluorobenzene BWG0844-MS1 Toluene-dB BWG0844-MSD1 1,2-Dichloroethane-d4 BWG0844-MSD1 4-Bromofluorobenzene BWG0844-MSD1 Toluene-dB CtF WO#: 22G1280 www.ChemtechFord.com %Rec LCL UCL Result Blank -EPA 8260D /5030A 111 64.2 126 11.1 102 71.4 122 10.2 102 63.2 129 10.2 LCS -EPA 8260D /5030A 107 64.2 126 10.7 108 71.4 122 10.8 103 63.2 129 10.3 Matrix Spike -EPA 8260D /5030A 104 64.2 126 10.4 104 71.4 122 10.4 100 63.2 129 10.0 Matrix Spike Dup -EPA 8260D /5030A 104 64.2 126 10.4 108 71.4 122 10.8 100 63.2 129 10.0 Spk Value Batch OF 10.0 BWG0844 1.00 10.0 BWG0844 1.00 10.0 BWG0844 1.00 10.0 BWG0844 1.00 10.0 BWG0844 1.00 10.0 BWG0844 1.00 10.0 BWG0844 1.00 10.0 BWG0844 1.00 10.0 BWG0844 1.00 10.0 BWG0844 1.00 10.0 BWG0844 1.00 10.0 BWG0844 1.00 Page 38 of 40 Surrogate Recoveries (Field Samples) LabNumber Analyte 8260 Low Level Volatiles 22G1280-01 4-Bromofluorobenzene 22G1280-01 Toluene-dB 22G1280-01 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22G1280-02 1,2-Dichloroethane-d4 22G1280-02 22G1280-02 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22G 1280-03 1,2-Dichloroethane-d4 22G1280-03 22G1280-03 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22G 1280-04 1,2-Dichloroethane-d4 22G1280-04 22G1280-04 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22G1280-05 Toluene-dB 22G1280-05 22G1280-05 1,2-Dichloroethane-d4 4-Bromofluorobenzene 8260 Low Level Volatiles 22G1280-06 4-Bromofluorobenzene 22G1280-06 22G1280-06 Toluene-dB 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22G1280-07 1,2-Dichloroethane-d4 22G1280-07 22G1280-07 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22G 1280-08 1,2-Dichloroethane-d4 22G1280-08 4-Bromofluorobenzene CtF WO#: 22G1280 www.ChemtechFord.com Result 10.5 10.0 10.3 10.2 10.2 10.0 10.4 10.2 10.3 10.2 10.1 10.0 10.2 10.2 10.3 10.2 10.0 10.4 10.5 9.89 10.0 11.2 10.1 SpkLvl 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 %Rec 105 100 103 102 102 100 104 102 103 102 101 100 102 102 103 102 100 104 105 98.9 100 112 101 LCL UCL 71.4 122 63.2 129 64.2 126 64.2 126 71.4 122 63.2 129 64.2 126 71.4 122 63.2 129 64.2 126 71.4 122 63.2 129 63.2 129 64.2 126 71.4 122 71.4 122 63.2 129 64.2 126 64.2 126 71.4 122 63.2 129 64.2 126 71.4 122 Qualifier Page 39 of 40 22G1280-08 Toluene-dB 8260 Low Level Volatiles 22G1280-09 1,2-Dichloroethane-d4 22G1280-09 22G1280-09 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22G1280-10 Toluene-dB 22G1280-10 22G1280-10 1,2-Dichloroethane-d4 4-Bromofluorobenzene CtF WO#: 22G1280 www.ChemtechFord.com 10.0 10.6 9.87 10.2 10.0 10.9 10.2 10.0 10.0 10.0 10.0 10.0 10.0 10.0 100 106 98.7 102 100 109 102 63.2 129 64.2 126 71.4 122 63.2 129 63.2 129 64.2 126 71.4 122 Page 40 of 40 Client Service Contact: 801.262.7299 �� Serving the lntermountain West since 1953 Page 1 of 36 CHEMTECH-FORD LABORATORIES Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2022 Project Manager: Tanner Holliday ·Laboratory ID 22G1743-01 22G1743-02 22G1743-03 22G1743-04 22G1743-05 22G1743-06 22G1743-07 22G1743-08 22G1743-09 22G1743-10 Sample Name MW-12_07142022 MW-27 _07152022 MW-28_07152022 MW-29_07142022 MW-32_07152022 MW-24A_07192022 MW-24_07202022 MW-38 _ 07202022 MW-65 _ 07202022 Trip Blank Work Order Report Narrative Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions There are no corrective actions associated with this work order. Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 22G1743 Page 2 of 36 CHEMTECH·FORD LA60�.,\TORIE5 Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com Certificate of Analysis Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations ND = Not detected at the corresponding Minimum Reporting Limit (MRL). PO#: Receipt: 1121122 11:40@0.1 ·c Date Reported: 8/12/2022 Project Name: 3rd Quarter Ground Water 2022 I mg/L = one milligram per liter or I mg/kg = one milligram per kilogram = I part per million. 1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion. I ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion Project Name: 3rd Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 22G1743 Page 17 of 36 Client Address: Contact Phone#: Email: Project Name: Project#: PO#: Sampler Name: IIW-12_ OT14::il022 IIIW-27_071112022 .� IIW-28_071112m2 ( 11111'-29 071420'1.2 ' - ,� IIW-32_0T152m'l 8 7 a � 10 11 12 American West Analytical Laboratories 463W.3600S. Saltl..akeetty,UT B4115 Phone# (801) 263-8686 Toi Free# (888) 263-8686 Fax # (801 ) 263-8687 Email awal@awal-labs.com www.awal-labs.com Energy Fuels Resources, Inc. 6425 S. Hwy. 191 Blanding, UT 84511 Tanner Holliday (435) 678-2221 Cell#: u.o111..,,.-�-- -�mufa .... _ 3rd Quarter Ground Water 2022 Tanner Holliday Date Samole ID: SamnlAII 7/14/2m2 7/1S/2m2 7/15/2m'l 7/14/2m'l 7/111/202'1. •--by. _-, _ __,. p-�-., -/Cleta; .......... _ 7 -, V o,m,,: .... _, T.,,,,.ru,.s,t_, "" R-by. DIii: .,......,_ r.,,., P,..Nome: R--by. .,.,.,, L<a-.. lino: P,HNo-: .......--by. .,..,, le_,_ , ... , ...... _ CHAIN OF CUSTODY Al •,_lysla will be condudllld laing NElAP ■caedied mathoda en:::I ■I data wil be reported using AWAL'• standard ■1111� lilla and reporting limits (PQL) � speciflcaly ,equnled oa.w.. on U. Chlin a( Cl.atody end/or attached doct.merU.lion AWAL lab Sample Set# Page 1 of 2 QCL8Y81: 3 "" o'0 � c:, 0) f! � ... .. -g 0 C 8 5 � C ls I!: � -! :!:.Time 0 s 'l5 E 0 SamnlM .. I!: .. f/J 1240 I w 1045 2 w X 1435 3 w X X 1320 I w 1220 I w X ,._by. ... t>rirCNalft9:' ��, h ,.,,__ r/L-..,, �"It) t!.• � .,,..NJimo: > /evr "'-�:, h,_,/1,,-.:, R--i,y. ' L•---tuw .,.,._ •-by. s-.. Pl'4rifNama· iii' iii' ii)' c;; c;; 0 c:, c:, 0 "' "' "' 1:::-;::: ----....0 g g c:, � t!. � a I 9 .e ii.e "lJ i ::, '11 '11 '11 !! i0 0 ,; ,; aQ Q X X X X X _/ C---..... / I Tum Around Time: Unlasa other ■l'Tllngem■nta t,e,.. bNn made, Due Date: __ ,..be.......,by5:00pmon Standard the day they mt due X lndude EDD: Laboraloly Use Orly L0CUll UPLOAD UCBL is,.,,,,,...w...,, )( Field Filtered For: l>laom,,ll(ebla SNppoc10<hond- � ii)' Am-era-g For Compliance With: (1(. 1-c ci iic c:, 0 NELAP "' 0 T--"' ----□RCRA ;::: .... 0 0 "' □CWA R-B-kslg c ----c:, 0 .... □SOWA Ompn,perly Soudl t!. � 0 □ELAP/A2LA g 0 y N i c' � 0 NUAP c o' ' ;; 'ii □Non-Compliance Pr-,y-c:, c 0) c:, g ... □01her. y N � ... 0) " ii Clwcudotbonc/1 0 II !!. c:, �y N '11 c:, '11 i" It) c:, " " !:!:. c:, ! ! Known Hazards -w-"' 0 0 � 0 a 0 Holdi,gTlmN ,; i a a & ' 1 y Q Samole Comments X -onO...PJtd<o;o y N NA �onO....Pocllago y N NA Preearl.onS.mpe. y N NA Unt:mken on S.mpte y N NA -S.mpa La-and C0C R-,r? y N .,...., Special Instructions: Time: Sample containers for metals were field liltCTed. See the r"'7 /.,2 I /1--1..-Analytical Scope of Work for Reporting Limits end voe anaJyte ime: 1/L.fn lisL �le: rnno """'' rr..,., UPS GROUND TRACKING #: 1 z 187 y 4Y 03 9650 9187 Page 18 of 36 ·-.......... , � Client: Address: Contact: Phone#: Email: Project Name: Project#: PO#: Sampler Name: American West Analytical Laboratories 463 W, 3600 S. Salt Lake City. UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263--8686 Fax# (601) 263-8687 Email awal@awal-labs.com www.awal-labs.com Energy Fuels Resources, Inc. 6425 S. Hwy. 191 Blaadln.g, UT 84511 TaDDer Holliday (435) 678-2221 Cell#: tholHda�eaeq;Jfaela.com; ll:wemel@eneqJfaela.com. 3rd Quarter Ground Water 2022 TaDDer Holliday Date SamolelD: Samoled d (f � IIW-24A_07192022 7/19/2022 r] � :.. >1 ,€ 6 8 9 10 ,, 12 IIW-24_07202022 IIW-38_07202022 IIW-615_07202022 Trip Blank �elinql-by. ..::J ""-nabn _.,,. ... .JJ.. 11 · L,,_ __ Tamer......,_ �eiJnQ<hhedby. -- PmlName: R�by. - ....... l\lam.e: �ellnquished by. -- PrinC Name. 7/20/2022 7/20/20'n 7/20/2022 7/19/2022 ...,, � 7 rune: ffW '°""" rrme: Dale: nme: Date: ,me: I Time Samoled 700 810 830 830 700 CHAIN OF CUSTODY All analysis will be conducled using NELAP - method!! and all data will be reported using AWAL's slandarcl anaJyte lists and reporting limits (POL) unless specifically requested Olhefwlse on Im Chain or Cusllldy ancMor attached documentation. QC Level: I Tum Around Time: Uress olher arrangements have been made, signed reports wlll be emalled by 5:00 pm on 3 Standard the day they are rue � Include EDD: 0 LOCU8 UPLOAD :::;; C.> EXCEL oii oii X Field Filtered For: ::;; Dt.aolved. lletala .... vi ::;; ';:,t.- .0 <G � 0.. z For Compliance With: c i.i:D NELAP C N D RCRA o' C'I c � -;; >' D CWA C c () :i D SDWA � l") 0 -iii' C 0 ELAP/A2lA .. a C.> i: 0 □NLLAP 1/) C � C c-. -; ,: D Non-Compliance l") C l") () ¢ :;i .. 1/) a .. D Other: 0 :it. •.,;� ; � c:, G' = :a () oii •C .... C < Cl IC C :s (') C i 1 .; .; I !! m 0 1/) � ii a) 1/) .t Cl) � Known Hazards ls I: :it. a .. -u -0 ri z • u a. s (') CD = : <8 E = c � IS .. .,i I: I: u Q 0 >Samele Comments ... 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 3 w X Recelvod by< i,A ,_,, t.h .. �/ 71/i.//,z...L-..... Special Instructions: AWAL Lab Sample Set# Page 2 of 2 Due Date: laboratory Use Only is-,,p1es Wen,: 1 5tlppod or hand � 2 Amb4ent or Chilled 3 Tempermn <.4--( ·c 4 R--� (lm-1)--) y 5 Prope<ly-y N Ched<edatbencll y N 6 -- Ho4dlng Times y COC Tape Was: , Presarf on OUlerPacl<age y N NA 2 lJnbmlcen on OUler Package y N 3 Presenl on Sanple y N NA Unbmken on Sanple y N NA 8-lSanple '--aidCOCRea>nl? y N 2 /1,. �, .... Jh A�l-..J,__,I' rr1mo//t/(_; .,,.._ Sample containers for metals were field filtered. See the R....,._by. I Pate: -... Analytical Scope of Work for Reporting Umits and voe analyte 1nne: list. 0nnt.Name: Received by. Pate: ,,.,,_.,, jrrne: ""'""Name: �--by. !Date: -- 111me: Page 19 of 36 Print Name: Delivery Method: UPS o USPS D FedEx D Chemtech Courier o Walk-in o Customer Courier . 0lemtech Lot. Sample# Container Prwlln cl r.) l/ Y71 I I �- (J, , l-l ;✓-;/ / (J A,< // ::- o:-; C' �� ;11 I ( .,,. (i ,V / :;._ ,, / # r4 /l i .,.,.."'f .. ,.,.. ✓-· <"'__ ., i.) �A c/,.._f r ()(,. -C.:·"', VV}Cf.,ii :S-& JV G__,1-::.. / le ' II I/, '"- i_;l ,.,.• � /i f::'C fl t1 i..::. (, \'t -I- ll'-'U) JJ.. c) /J wC A-, ·,/4 ( I i I I i �II I :i J :& :!Ii! a i .s ll. Misc ,s ' .B 1 Volume J f s 101/ml.l CHEMTECH FORD LABORATORIES Sample Receipt Receiving Temperature / oc I -. -� ; - Comments CHEMTECH-FORD l.,\BQRt,TOPl,·5 Sample Condition (check if yes) Containers Intact COC an be matched to bottles Received on Ice Suff1cent Sample Volume D Headspace Present (VOC) 0 lemperature Blank [Z] Received within Holding Time "lastk: Containers A- PlaJtic l/nprue,vcd a.. Miscellaneous Plastic C· Cyanide Qt (NaOH) E • Coliform/Ecoli/H PC F-Sulfide Qt (Zn Acetate) l· Mercury 1631 M• Metals Pint (HND3) N• Nutrient Pint (H2S04) R· Radiological (HND3) S· Sludge Cups/Tubs Q• Plastic Bag Glass Containers D· 625 (Na2S203) G· Glass Unpreserved H· HAAs (NH4CI) J-508/SJS/S2S (Na2S03) K- 51S.3 Herbicides O· Oil & Grease (HCI) P- Phenols (H2S04) T · TOC/TOX (H3PD4) U- 531 (MCAA, Na2S203) V- S24/THMs (Ascorbic Acid) W- 8260 voe (1:1 HCI) X-Vial Unpreserved Y- 624/S04 (Na2S203) Z-Miscellaneous Glass Page 20 of 36 QC Report for Work Order (WO) -22G1743 Analyte % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank - EPA 200.7 QC Sample ID: BWH0230-BLK1 Batch: BWH0230 Date Prepared: 08/03/2022 Date Analyzed: 08/03/2022 Calcium, Dissolved ND 0.2 1.00 Iron, Dissolved ND 0.03 1.00 Magnesium, Dissolved ND 0.2 1.00 Potassium, Dissolved ND 0.5 1.00 Sodium, Dissolved ND 0.5 1.00 Tin, Dissolved ND 0.10 1.00 QC Sample ID: BWH0702-BLK1 Batch: BWH0702 Date Prepared: 08/11/2022 Date Analyzed: 08/11/2022 Calcium, Dissolved ND 0.2 1.00 Sodium, Dissolved ND 0.5 1.00 LCS -EPA 200. 7 QC Sample ID: BWH0230-BS1 Batch: BWH0230 Date Prepared: 08/03/2022 Date Analyzed: 08/03/2022 Calcium, Dissolved 102 85 -115 10.4 10.2 0.2 1.00 Iron, Dissolved 117 85 -115 0.234 0.200 0.02 1.00 QM-11 -The Laboratory Control Sample recovery was outside acceptance limits. The analytical batch was accepted based on the recovery of the Method Spike. Magnesium, Dissolved 106 85 -115 10.9 10.2 0.2 1.00 Potassium, Dissolved 107 85 -115 10.7 10.0 0.5 1.00 Sodium, Dissolved 104 85 -115 10.4 10.0 0.5 1.00 Tin, Dissolved 102 85 -155 0.20 0.200 0.02 1.00 QC Sample ID: BWH0702-BS 1 Batch: BWH0702 Date Prepared: 08/11/2022 Date Analyzed: 08/11/2022 Calcium, Dissolved 90.6 85 -115 9.2 10.2 0.2 1.00 Sodium, Dissolved 93.4 85 -115 9.3 10.0 0.5 1.00 Matrix Spike -EPA 200. 7 QC Sample ID: BWH0230-MS1 Batch: BWH0230 QC Source Sample: 22G 1743-07 Date Prepared: 08/03/2022 Date Analyzed: 08/03/2022 Calcium, Dissolved -608 70 -130 401 463 10.2 0.2 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Iron, Dissolved 85.8 70 -130 0.177 0.006 0.200 0.02 1.00 Magnesium, Dissolved 146 70 -130 179 164 10.2 0.2 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Potassium, Dissolved 91.6 70 -130 20.1 10.9 10.0 0.5 1.00 Sodium, Dissolved -797 70 -130 361 441 10.0 0.5 1.00 Tin, Dissolved 78.3 70 -130 0.16 0.004 0.200 0.02 1.00 QC Sample ID: BWH0230-MS2 Batch: BWH0230 QC Source Sample: 22Gl 743-08 Date Prepared: 08/03/2022 Date Analyzed: 08/03/2022 Calcium, Dissolved 116 70 -130 473 461 10.2 0.2 1.00 Iron, Dissolved 105 70-130 0.210 ND 0.200 0.02 1.00 Magnesium, Dissolved 106 70-130 200 190 10.2 0.2 1.00 Potassium, Dissolved 96.3 70 -130 36.2 26.6 10.0 0.5 1.00 Sodium, Dissolved -30.8 70 -130 384 387 10.0 0.5 1.00 CtF WO#: 22G1743 www.ChemtechFord.com Page 21 of 36 Analyte QC Sample ID: BWH0230-MS2 Date Prepared: 08/03/2022 QC Report for Work Order (WO) -22G1743 %Rec RPD Limits RPD Max Result Source Cone Matrix Spike -EPA 200.7 (cont.) Batch: BWH0230 QC Source Sample: 22G 1743-08 Date Analyzed: 08/03/2022 Spk Value MRL QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Tin, Dissolved 97.6 70 -130 0.20 ND 0.200 0.02 QC Sample ID: BWH0702-MS1 Batch: BWH0702 QC Source Sample: 2201743-07 Date Prepared: 08/11/2022 Date Analyzed: 08/11/2022 Calcium, Dissolved 80.3 70 -130 545 463 102 2.0 Sodium, Dissolved 75.8 70 -130 516 441 100 5.0 Matrix Spike Dup -EPA 200.7 QC Sample ID: BWH0230-MSD1 Batch: BWH0230 QC Source Sample: 2201743-07 Date Prepared: 08/03/2022 Date Analyzed: 08/03/2022 Calcium, Dissolved -614 0.144 70 -130 20 400 463 10.2 0.2 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. DF 1.00 1.00 1.00 1.00 lron,Dissolved 94.0 8.89 70-130 20 0.194 0.006 0.200 0.02 1.00 Magnesium, Dissolved 136 0.558 70 -130 20 178 164 10.2 0.2 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Potassium, Dissolved Sodium, Dissolved 88.7 -891 1.43 2.65 70 -130 70 -130 20 20 19.8 351 10.9 441 10.0 10.0 0.5 0.5 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Tin, Dissolved QC Sample ID: BWH0230-MSD2 Date Prepared: 08/03/2022 Calcium, Dissolved 82.3 4.86 70 -130 20 0.17 Batch: BWH0230 QC Source Sample: 22G 1743-08 Date Analyzed: 08/03/2022 385 5.62 70 -130 20 501 0.004 0.200 0.02 461 10.2 0.2 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Iron, Dissolved 109 4.11 70 -130 20 0.219 ND 0.200 0.02 Magnesium, Dissolved 218 5.52 70 -130 20 212 190 10.2 0.2 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Potassium, Dissolved 114 4.82 70 -130 20 38.0 26.6 10.0 0.5 Sodium, Dissolved 130 4.09 70 -130 20 400 387 10.0 0.5 Tin, Dissolved 105 7.21 70 -130 20 0.21 ND 0.200 0.02 QC Sample ID: BWH0702-MSD1 Batch: BWH0702 QC Source Sample: 22G 1743-07 Date Prepared: 08/11/2022 Date Analyzed: 08/11/2022 Calcium, Dissolved 51.9 5.47 70 -130 20 516 463 102 2.0 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 Sodium, Dissolved 49.6 5.21 70 -130 20 490 441 100 5.0 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. CtF WO#: 22G1743 www.ChemtechFord.com Page 22 of 36 QC Report for Work Order (WO) -22G1743 Analyte % Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Blank -EPA 200.8 QC Sample ID: BWH0023-BLK1 Batch: BWH0023 Date Prepared: 08/01/2022 Date Analyzed: 08/01/2022 Arsenic, Dissolved ND 0.0050 1.00 Beryllium, Dissolved ND 0.0005 1.00 Cadmium, Dissolved ND 0.0005 1.00 Chromium, Dissolved ND 0.0250 1.00 Cobalt, Dissolved ND 0.010 1.00 Copper, Dissolved ND 0.0100 1.00 Lead, Dissolved ND 0.0010 1.00 Manganese, Dissolved ND 0.0100 1.00 Molybdenum, Dissolved ND 0.0100 1.00 Nickel, Dissolved ND 0.0200 1.00 Selenium, Dissolved ND 0.0050 1.00 Silver, Dissolved ND 0.010 1.00 Thallium, Dissolved ND 0.0005 1.00 Uranium, Dissolved ND 0.0003 1.00 Vanadium, Dissolved ND 0.0150 1.00 Zinc, Dissolved ND 0.01 1.00 LCS -EPA 200.8 QC Sample ID: BWH0023-BS 1 Batch: BWH0023 Date Prepared: 08/01/2022 Date Analyzed: 08/01/2022 Arsenic, Dissolved 98.7 85 -115 0.039 0.0400 0.0005 1.00 Beryllium, Dissolved 101 85 -115 0.040 0.0400 0.0005 1.00 Cadmium, Dissolved 97.4 85 -115 0.039 0.0400 0.0002 1.00 Chromium, Dissolved 97.8 85 -115 0.039 0.0400 0.0005 1.00 Cobalt, Dissolved 95.4 85 -115 0.038 0.0400 0.0005 1.00 Copper, Dissolved 93.5 85 -115 0.037 0.0400 0.0010 1.00 Lead, Dissolved 102 85 -115 0.041 0.0400 0.0005 1.00 Manganese, Dissolved 97.2 85 -115 0.039 0.0400 0.0005 1.00 Molybdenum, Dissolved 99.0 85 -115 0.040 0.0400 0.0005 1.00 Nickel, Dissolved 94.0 85 -115 0.0376 0.0400 0.0005 1.00 Selenium, Dissolved 98.7 85 -115 0.039 0.0400 0.0005 1.00 Silver, Dissolved 97.7 85 -115 0.039 0,0400 0.0005 1.00 Thallium, Dissolved 109 85 -115 0.044 0.0400 0.0002 1.00 Uranium, Dissolved 106 85 -115 0.042 0.0400 0.0003 1.00 Vanadium, Dissolved 97.9 85 -115 0.039 0.0400 0.0005 1.00 Zinc, Dissolved 96.2 85 -115 0.04 0.0400 0.01 1.00 Matrix Spike -EPA 200.8 QC Sample JD: BWH0023-MS1 Batch: BWH0023 QC Source Sample: 22G 1743-07 Date Prepared: 08/01/2022 Date Analyzed: 08/01/2022 Arsenic, Dissolved 100 70 -130 0.040 ND 0.0400 0.0005 1.00 Beryllium, Dissolved 91.0 70 -130 0.039 0.003 0.0400 0.0005 1.00 Cadmium, Dissolved 91.1 70 -130 0.045 0.009 0.0400 0.0002 1.00 Chromium, Dissolved 90.5 70 -130 0.037 0.0006 0.0400 0.0005 1.00 Cobalt, Dissolved 82.2 70 -130 0.146 0.113 0.0400 0.0005 1.00 Copper, Dissolved 79.8 70 -130 0.046 0.014 0.0400 0.0010 1.00 Lead, Dissolved 91.9 70 -130 0.039 0.002 0.0400 0.0005 1.00 Manganese, Dissolved -2440 70 -130 6.56 7.54 0.0400 0.0005 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Molybdenum, Dissolved 104 70 -130 0.042 0.0002 0.0400 0.0005 1.00 CtF WO#: 22G1743 www.ChemtechFord.com Page 23 of 36 Analyte QC Sample ID: BWH0023-MS1 Date Prepared: 08/01/2022 Nickel, Dissolved Selenium, Dissolved Silver, Dissolved Thallium, Dissolved Uranium, Dissolved Vanadium, Dissolved Zinc, Dissolved QC Sample ID: BWH0023-MS2 Date Prepared: 08/01/2022 Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Lead, Dissolved Manganese, Dissolved Molybdenum, Dissolved Nickel, Dissolved Selenium, Dissolved Silver, Dissolved Thallium, Dissolved Uranium, Dissolved Vanadium, Dissolved Zinc, Dissolved CtF WO#: 22G1743 www.ChemtechFord.com QC Report for Work Order (WO) -22G1743 % Rec RPD Limits RPD Max Result Source Cone SpkValue MRL DF Matrix Spike - EPA 200.8 (cont.) Batch: BWH0023 QC Source Sample: 22G 1743-07 Date Analyzed: 08/01/2022 77.0 75 -125 0.101 0.0699 0.0400 0.0005 1.00 103 70-130 0.055 0.014 0.0400 0.0005 1.00 87.7 70 -130 0.035 ND 0.0400 0.0005 1.00 98.9 70 -130 0.043 0.003 0.0400 0.0002 1.00 101 70-130 0.047 0.007 0.0400 0.0003 1.00 96.4 70 -130 0.039 0.0003 0.0400 0.0005 1.00 73.0 70 -130 0.14 0.11 0.0400 0.01 1.00 Batch: BWH0023 QC Source Sample: 22G 1743-08 Date Analyzed: 08/01/2022 103 70 -130 0.041 ND 0.0400 0.0005 1.00 90.0 70-130 0.036 ND 0.0400 0.0005 1.00 95.2 70 -130 0.038 0.00008 0.0400 0.0002 1.00 97.6 70 - 130 0.040 0.0007 0.0400 0.0005 1.00 93.7 70 -130 0.038 0.0005 0.0400 0.0005 1.00 87.2 70 -130 0.038 0.003 0.0400 0.0010 1.00 96.8 70 -130 0.039 ND 0.0400 0.0005 1.00 95.4 70 -130 0.039 0.001 0.0400 0.0005 1.00 107 70 -130 0.051 0.008 0.0400 0.0005 1.00 89.1 75 -125 0.0383 0.0027 0.0400 0.0005 1.00 102 70 -130 0.197 0.156 0.0400 0.0005 1.00 84.5 70 -130 0.034 0.0002 0.0400 0.0005 1.00 99.5 70 -130 0.040 0.0001 0.0400 0.0002 1.00 108 70 -130 0.049 0.006 0.0400 0.0003 1.00 102 70 -130 0.041 0.0006 0.0400 0.0005 1.00 87.2 70 -130 0.04 0.003 0.0400 0.01 1.00 Page 24 of 36 Analyte QC Sample ID: BWG 1118-BLK I Date Prepared: 07/22/2022 Mercury, Dissolved QC Sample ID: BWG1118-BS1 Date Prepared: 07/22/2022 Mercury, Dissolved QC Sample ID: BWGI 118-MSl Date Prepared: 07/22/2022 Mercury, Dissolved QC Sample ID: BWG l ll 8-MS3 Date Prepared: 07/22/2022 Mercury, Dissolved QC Sample ID: BWG I I 18-MS4 Date Prepared: 07/22/2022 Mercury, Dissolved QC Sample ID: BWG 1118-MSD I Date Prepared: 07/22/2022 Mercury, Dissolved QC Sample ID: BWG I I I 8-MSD3 Date Prepared: 07/22/2022 Mercury, Dissolved QC Sample ID: BWG1118-MSD4 Date Prepared: 07/22/2022 Mercury, Dissolved CtF WO#: 22G1743 www.ChemtechFord.com QC Report for Work Order (WO) -22G1743 % Rec RPO Limits RPO Max Result Source Cone Blank -EPA 245.1 Batch:BWG1118 Date Analyzed: 07/26/2022 ND LCS -EPA 245.1 Batch: BWGl 118 Date Analyzed: 07/26/2022 114 85 -115 0.00570 Matrix Spike - EPA 245.1 Batch: BWG1118 QC Source Sample: XXXXXXX-XX Date Analyzed: 07/27/2022 111 75 -125 0.00556 ND Batch: BWG 1118 QC Source Sample: 22G 1743-07 Date Analyzed: 07/27/2022 114 75 -125 0.00572 ND Batch: BWG 1118 QC Source Sample: 22G 1743-08 Date Analyzed: 07/27/2022 112 75 -125 0.00561 ND Matrix Spike Dup -EPA 245.1 Batch: BWG 1118 QC Source Sample: XXXXXXX-XX Date Analyzed: 07/27/2022 107 3.53 75 -125 20 0.00536 ND Batch: BWG1118 QC Source Sample: 22G 1743-07 Date Analyzed: 07/27/2022 109 4.86 75 -125 20 0.00544 ND Batch: BWG1118 QC Source Sample: 2201743-08 Date Analyzed: 07/27/2022 110 1.86 75 -125 20 0.00551 ND Spk Value MRL OF J.0005(1.00 0.00500 l0001E 1.00 0.00500 l0001E 1.00 0.00500 J.0001E 1.00 0.00500 J.0001E 1.00 0.00500 l0001E 1.00 0.00500 l0001E 1.00 0.00500 J.0001E 1.00 Page 25 of 36 QC Report for Work Order (WO) -22G1743 Analyte %Rec RPD Limits RPD Max Result Source Cone SpkValue MRL Blank -EPA 300.0 QC Sample ID: BWGI039-BLKI Batch: BWGI039 Date Prepared: 07/21/2022 Date Analyzed: 07/22/2022 Chloride ND 1.0 Fluoride ND 0.100 Sulfate ND 1.0 QC Sample ID: BWGl 113-BLKl Batch: BWGI 113 Date Prepared: 07/22/2022 Date Analyzed: 07/22/2022 Chloride ND 1.0 Fluoride ND 0.100 Sulfate ND 1.0 QC Sample ID: BWGI I 75-BLKl Batch: BWG1175 Date Prepared: 07/26/2022 Date Analyzed: 07/26/2022 Sulfate ND 1.0 QC Sample ID: BWH0714-BLK1 Batch: BWH0714 Date Prepared: 08/11/2022 Date Analyzed: 08/12/2022 Chloride ND 1.0 LCS -EPA 300.0 QC Sample ID: BWGI039-BS1 Batch: BWG1039 Date Prepared: 07/21/2022 Date Analyzed: 07/22/2022 Chloride 103 90 -110 51.5 50.0 1.0 Fluoride 99.5 90 -110 4.97 5.00 0.100 Sulfate 98.6 90 -110 49.3 50.0 1.0 QC Sample ID: BWG1113-BS1 Batch: BWGI 113 Date Prepared: 07/22/2022 Date Analyzed: 07/22/2022 Chloride 103 90 -110 51.6 50.0 1.0 Fluoride 94.0 90 -110 4.70 5.00 0.100 Sulfate 98.9 90 -110 49.4 50.0 1.0 QC Sample ID: BWGl 175-BSI Batch: BWG I I 75 Date Prepared: 07/26/2022 Date Analyzed: 07/26/2022 Sulfate 98.1 90 -110 49.0 50.0 1.0 QC Sample ID: BWH0714-BS1 Batch: BWH0714 Date Prepared: 08/11/2022 Date Analyzed: 08/12/2022 Chloride 101 90 - 110 50.5 50.0 1.0 Matrix Spike -EPA 300.0 QC Sample ID: BWG1039-MS1 Batch: BWG1039 QC Source Sample: 22G 1743-07 Date Prepared: 07/21/2022 Date Analyzed: 07/22/2022 Chloride 102 80 -120 148 46.2 100 11.0 Fluoride 90.3 80 -120 9.79 0.760 10.0 1.10 Sulfate 266 80 -120 3070 2800 100 11.0 E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWG1039-MS2 Date Prepared: 07/21/2022 Chloride Fluoride Batch: BWG1039 QC Source Sample: 2201743-08 Date Analyzed: 07/22/2022 103 80 -120 63.7 80 -120 147 6.66 44.5 0.291 100 10.0 11.0 1.10 DF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 CtF WO#: 22G1743 www. Chem tech Ford. com Page 26 of 36 Analyte QC Sample ID: BWG1039-MS2 Date Prepared: 07/21/2022 QC Report for Work Order (WO) -22G1743 % Rec RPO Limits RPO Max Result Source Cone Matrix Spike -EPA 300.0 (cont.) Batch: BWG1039 QC Source Sample: 22Gl743-08 Date Analyzed: 07/22/2022 Spk Value MRL QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. Sulfate 312 80 -120 2800 2490 100 11.0 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). QC Sample ID: BWG 1113-MS 1 Batch: BWG 1113 QC Source Sample: 22G 1743-07 Date Prepared: 07/22/2022 Chloride Fluoride Sulfate QC Sample ID: BWG11I3-MS2 Date Prepared: 07/22/2022 Chloride Fluoride Sulfate QC Sample ID: BWGl 175-MSl Date Prepared: 07/26/2022 Sulfate QC Sample ID: BWG 1 l 75-MS2 Date Prepared: 07/26/2022 Sulfate QC Sample ID: BWH0714-MS1 Date Prepared: 08/11/2022 Chloride QC Sample ID: BWH0714-MS2 Date Prepared: 08/11/2022 Chloride QC Sample ID: BWG1039-MSD1 Date Prepared: 07 /2 l /2022 Chloride Fluoride Sulfate Date Analyzed: 07/22/2022 98.8 80 -120 1030 40.7 82.0 80 -120 82.0 ND 103 80 -120 3830 2800 Batch: BWGll 13 QC Source Sample: 22G 1743-08 Date Analyzed: 07/22/2022 98.1 80 -120 1030 44.5 80.0 80 -120 80.0 ND 103 80 -120 3530 2490 Batch: BWGl 175 QC Source Sample: XXXXXXX-XX Date Analyzed: 07/26/2022 98.2 80 -120 285 187 Batch: BWGl 175 QC Source Sample: XXXXXXX-XX Date Analyzed: 07/26/2022 88.2 80 -120 90.9 2.7 Batch: BWH0714 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/12/2022 109 80 -120 359 250 Batch: BWH0714 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/12/2022 387 80 -120 387 Matrix Spike Dup -EPA 300.0 Batch: BWG1039 QC Source Sample: 22G 1743-07 Date Analyzed: 07/22/2022 101 0.577 80 -120 20 147 46.2 91.6 1.37 80 • 120 20 9.92 0.760 234 1.03 80 -120 20 3040 2800 1000 110 100 11.0 1000 110 1000 110 100 11.0 1000 110 100 11.0 100 11.0 100 11.0 100 11.0 100 11.0 10.0 1.10 100 11.0 E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWG1039-MSD2 Date Prepared: 07/21/2022 Chloride Fluoride Batch: BWG1039 QC Source Sample: 22G 1743-08 Date Analyzed: 07/22/2022 102 0.758 80 • 120 64.5 1.18 80 -120 20 20 146 6.74 44.5 0.291 100 10.0 11.0 1.10 OF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 CtF WO#: 22G1743 www.ChemtechFord.com Page 27 of 36 Analyte QC Sample ID: BWG1039-MSD2 Date Prepared: 07/21/2022 QC Report for Work Order (WO) -22G1743 % Rec RPO Limits RPO Max Result Source Cone Matrix Spike Dup - EPA 300.0 (cont.) Batch: BWG1039 QC Source Sample: 22Gl743-08 Date Analyzed: 07/22/2022 Spk Value MRL QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. Sulfate 301 0.364 80 - 120 20 2790 2490 100 11.0 E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWG 1113-MSDI Batch: BWG1113 QC Source Sample: 22G 1743-07 Date Prepared: 07/22/2022 Date Analyzed: 07/22/2022 Chloride 99.1 0.335 80 -120 20 1030 40.7 1000 Fluoride 80.5 1.92 80 - 120 20 80.5 ND 100 Sulfate 103 0.117 80 - 120 20 3830 2800 1000 QC Sample ID: BWGlll3-MSD2 Batch: BWGI 113 QC Source Sample: 22G 1743-08 Date Prepared: 07/22/2022 Date Analyzed: 07/22/2022 Chloride 96.9 1.15 80 - 120 20 1010 44.5 1000 Fluoride 77.2 3.55 80 -120 20 77.2 ND 100 QM-12 -The MSD recovery was outside acceptance limits, but passed duplicate spike acceptance criteria. The batch was accepted based on the acceptability of the MS. Sulfate QC Sample ID: B WG 1175-MSD I Date Prepared: 07/26/2022 Sulfate QC Sample ID: BWG1175-MSD2 Date Prepared: 07/26/2022 Sulfate QC Sample ID: BWH0714-MSD1 Date Prepared: 08/11/2022 Chloride QC Sample ID: BWH0714-MSD2 Date Prepared: 08/11/2022 Chloride 101 0.599 80 -120 20 3500 2490 Batch: BWG 1175 QC Source Sample: XXXXXXX-XX Date Analyzed: 07/26/2022 99.4 0.431 80 -120 20 286 187 Batch: BWG1175 QC Source Sample: XXX:XXXX-XX Date Analyzed: 07/26/2022 90.4 2.44 80 -120 20 93.1 2.7 Batch: BWH0714 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/12/2022 106 0.866 80 -120 20 356 250 Batch: BWH0714 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/12/2022 388 0.226 80 - 120 20 388 1000 100 100 100 100 110 11.0 110 110 11.0 110 11.0 11.0 11.0 11.0 OF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 CtF WO#: 22G1743 www.ChemtechFord.com Page 28 of 36 Analyte QC Sample ID: BWG\206-BLKl Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWG1206-BS1 Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWG1206-MS1 Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWG1206-MS2 Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWG 1206-MS3 Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWG1206-MSD1 Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWGl206-MSD2 Date Prepared: 07/26/2022 Ammonia as N QC Sample ID: BWG1206-MSD3 Date Prepared: 07/26/2022 Ammonia as N CtF WO#: 22G1743 www.ChemtechFord.com QC Report for Work Order (WO) -22G1743 % Rec RPO Limits RPO Max Result Source Cone Blank -EPA 350.1 Batch: BWG 1206 Date Analyzed: 07/26/2022 ND LCS -EPA 350.1 Batch: BWG1206 Date Analyzed: 07/26/2022 96.2 90 -110 0.962 Matrix Spike -EPA 350.1 Batch: BWG 1206 QC Source Sample: XXXXXXX-XX Date Analyzed: 07/26/2022 87.0 80-120 1.48 0.610 Batch: BWG 1206 QC Source Sample: 22G 1743-07 Date Analyzed: 07/26/2022 95.2 80 -120 1.06 0.104 Batch: BWG1206 QC Source Sample: 22G 1743-08 Date Analyzed: 07/26/2022 98.9 80 -120 0.989 ND Matrix Spike Dup - EPA 350.1 Batch: BWG1206 QC Source Sample: XXXXXXX-XX Date Analyzed: 07/26/2022 82.3 3.25 80 -120 20 1.43 0.610 Batch: BWG1206 QC Source Sample: 22G 1743-07 Date Analyzed: 07/26/2022 97.8 2.42 80 -120 20 1.08 0.104 Batch: BWG1206 QC Source Sample: 22G 1743-08 Date Analyzed: 07/26/2022 103 3.55 80 -120 20 1.03 ND SpkValue MRL OF 0.0500 1.00 1.00 0.0500 1.00 1.00 0.250 5.00 1.00 0.0500 1.00 1.00 0.0500 1.00 1.00 0.250 5.00 1.00 0.0500 1.00 1.00 0.0500 1.00 Page 29 of 36 QC Report for Work Order (WO) -22G1743 Analyte %Rec RPO Limits RPO Max Result Source Cone SpkValue Blank -EPA 353.2 QC Sample ID: BWGl417-BLK1 Batch: BWGl417 Date Prepared: 07/29/2022 Date Analyzed: 07/29/2022 Nitrate + Nitrite, Total, as N ND QC Sample ID: BWH0106-BLK1 Batch: BWH0106 Date Prepared: 08/02/2022 Date Analyzed: 08/02/2022 Nitrate + Nitrite, Total, as N ND LCS - EPA 353.2 QC Sample ID: BWG1417-BS1 Batch: BWG1417 Date Prepared: 07/29/2022 Date Analyzed: 07/29/2022 Nitrate + Nitrite, Total, as N 94.6 80 -120 1.89 2.00 QC Sample ID: BWHOI06-BSI Batch: BWH0106 Date Prepared: 08/02/2022 Date Analyzed: 08/02/2022 Nitrate + Nitrite, Total, as N 105 80 -120 2.10 2.00 Matrix Spike -EPA 353.2 QC Sample ID: BWGI417-MS1 Batch: BWG1417 QC Source Sample: 22G 1743-07 Date Prepared: 07/29/2022 Date Analyzed: 07/29/2022 Nitrate + Nitrite, Total, as N 92.5 80 -120 1.27 0.345 1.00 QC Sample ID: BWG1417-MS2 Batch: BWG1417 QC Source Sample: 22G 1743-08 Date Prepared: 07/29/2022 Date Analyzed: 07/29/2022 Nitrate+ Nitrite, Total, as N 90.2 80 -120 16.5 15.6 1.00 QC Sample ID: BWH0106-MSI Batch: BWH0106 QC Source Sample: 22G 1743-08 Date Prepared: 08/02/2022 Date Analyzed: 08/02/2022 Nitrate+ Nitrite, Total, as N 96.5 80 -120 15.3 14.4 1.00 QC Sample ID: BWH0106-MS2 Batch: BWH0106 QC Source Sample: XXXXXXX-XX Date Prepared: 08/02/2022 Date Analyzed: 08/02/2022 Nitrate + Nitrite, Total, as N 91.3 80 -120 5.95 5.04 1.00 Matrix Spike Dup -EPA 353.2 QC Sample ID: BWG1417-MSD1 Batch: BWG 1417 QC Source Sample: 22G 1743-07 Date Prepared: 07/29/2022 Date Analyzed: 07/29/2022 Nitrate + Nitrite, Total, as N 96.3 2.95 80 -120 20 1.31 0.345 1.00 QC Sample ID: BWG1417-MSD2 Batch: BWG1417 QC Source Sample: 22G 1743-08 Date Prepared: 07/29/2022 Date Analyzed: 07/29/2022 Nitrate+ Nitrite, Total, as N 70.7 1.19 80 -120 20 16.3 15.6 1.00 QM-12 -The MSD recovery was outside acceptance limits, but passed duplicate spike acceptance criteria. The batch was accepted based on the acceptability of the MS. QC Sample ID: BWH0106-MSD1 Date Prepared: 08/02/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWHOI06-MSD2 Date Prepared: 08/02/2022 Nitrate + Nitrite, Total, as N CtF WO#: 22G1743 www.ChemtechFord.com Batch: BWHOI06 QC Source Sample: 22G 1743-08 Date Analyzed: 08/02/2022 101 0.267 80 -120 20 15.4 14.4 Batch: BWH0106 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/02/2022 90.6 0.118 80 -120 20 5.94 5.04 1.00 1.00 MRL OF 0.100 1.00 0.100 1.00 0.100 1.00 0.100 1.00 0.100 1.00 0.100 1.00 1.00 10.00 0.500 5.00 0.100 1.00 0.100 1.00 1.00 10.00 0.500 5.00 Page 30 of 36 QC Report for Work Order (WO) -22G1743 Analyte % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -EPA 8260D /5030A QC Sample ID: BWH0006-BLK1 Batch: BWH0006 Date Prepared: 07/29/2022 Date Analyzed: 07/29/2022 Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 LCS -EPA 8260D /5030A QC Sample ID: BWH0006-BS1 Batch: BWH0006 Date Prepared: 07/29/2022 Date Analyzed: 07/29/2022 Acetone 86.0 70 -130 86.0 100 10.0 1.00 Benzene 105 70 -130 10.5 10.0 1.0 1.00 Carbon Tetrachloride 91.2 70 -130 9.12 10.0 1.0 1.00 Chloroform 121 70 -130 12.1 10.0 1.0 1.00 Chloromethane 90.3 70 -130 9.03 10.0 1.0 1.00 Methyl Ethyl Ketone 98.7 70 -130 98.7 100 10.0 1.00 Methylene Chloride 119 70 -130 11.9 10.0 1.0 1.00 Naphthalene 93.0 70 -130 9.30 10.0 1.0 1.00 Tetrahydrofuran 122 70 -130 12.2 10.0 1.0 1.00 Toluene 98.9 70 -130 9.89 10.0 1.0 1.00 Xylenes, total 102 70 -130 30.7 30.0 1.0 1.00 Matrix Spike -EPA 8260D /5030A QC Sample ID: BWH0006-MS1 Batch: BWH0006 QC Source Sample: 2201743-07 Date Prepared: 07/29/2022 Date Analyzed: 07/29/2022 Acetone 89.0 70-130 89.0 ND 100 10.0 1.00 Benzene 93.7 70 -130 9.37 ND 10.0 1.0 1.00 Carbon Tetrachloride 74.4 70 -130 7.44 ND 10.0 1.0 1.00 Chloroform 112 70 -130 11.2 ND 10.0 1.0 1.00 Chloromethane 74.1 70 -130 7.41 ND 10.0 1.0 1.00 Methyl Ethyl Ketone 98.3 70 -130 98.3 ND 100 10.0 1.00 Methylene Chloride 107 70 -130 10.7 ND 10.0 1.0 1.00 Naphthalene 84.0 70 -130 8.40 ND 10.0 1.0 1.00 Tetrahydrofuran 119 70 -130 11.9 ND 10.0 1.0 1.00 Toluene 86.7 70 -130 8.67 ND 10.0 1.0 1.00 Xylenes, total 91.2 70 -130 27.4 ND 30.0 1.0 1.00 Matrix Spike Dup - EPA 8260D /5030A QC Sample ID: BWH0006-MSDI Batch: BWH0006 QC Source Sample: 2201743-07 Date Prepared: 07/29/2022 Date Analyzed: 07/29/2022 Acetone 87.2 2.01 70 -130 20 87.2 ND 100 10.0 1.00 Benzene 94.5 0.850 70-130 20 9.45 ND 10.0 1.0 1.00 Carbon Tetrachloride 74.9 0.670 70 -130 20 7.49 ND 10.0 1.0 1.00 Chloroform 110 1.80 70 -130 20 11.0 ND 10.0 1.0 1.00 Chloromethane 75.3 1.61 70 -130 20 7.53 ND 10.0 1.0 1.00 Methyl Ethyl Ketone 97.1 1.21 70 -130 20 97.1 ND 100 10.0 1.00 Methylene Chloride 107 0.655 70 -130 20 10.7 ND 10.0 1.0 1.00 CtF WO#: 22G1743 www.ChemtechFord.com Page 31 of 36 Analyte QC Sample ID: BWH0006-MSD1 Date Prepared: 07/29/2022 Naphthalene Tetrahydrofuran Toluene Xylenes, total CtF WO#: 22G1743 www.ChemtechFord.com QC Report for Work Order (WO) -22G1743 %Rec RPO Limits RPO Max Result Source Cone Matrix Spike Dup -EPA 8260D /5030A (cont.) Batch: BWH0006 QC Source Sample: 2201743-07 Date Analyzed: 07/29/2022 87.6 4.20 70 -130 20 8.76 ND 124 4.37 70 -130 20 12.4 ND 87.8 1.26 70 -130 20 8.78 ND 92.9 1.85 70 -130 20 27.9 ND Spk Value MRL OF 10.0 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 30.0 1.0 1.00 Page 32 of 36 Analyte QC Sample ID: BWG1044-BLK1 Date Prepared: 07/21/2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) QC Sample ID: BWG1045-BLK1 Date Prepared: 07/21/2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) QC Sample ID: BWGJ044-DUP1 Date Prepared: 07/21/2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Alkalinity -Total (as CaCO3) QC Sample ID: BWG1045-DUPI Date Prepared: 07/21/2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Alkalinity -Total (as CaCO3) QC Sample ID: BWG1044-BSI Date Prepared: 07/21/2022 Alkalinity -Total (as CaCO3) QC Sample ID: BWG1045-BSI Date Prepared: 07/21/2022 Alkalinity -Total (as CaCO3) CtF WO#: 22G1743 www.ChemtechFord.com QC Report for Work Order (WO) -22G1743 % Rec RPD Limits RPO Max Result Source Cone Blank -SM 2320 B Batch: BWG1044 Date Analyzed: 07/21/2022 ND ND Batch: BWG1045 Date Analyzed: 07/21/2022 ND ND Duplicate -SM 2320 B Batch: BWG1044 QC Source Sample: 22G 1743-08 Date Analyzed: 07/21/2022 0.0973 20 103 103 20 ND ND 0.0973 20 103 103 Batch: BWG1045 QC Source Sample: 22Gl 743-07 Date Analyzed: 07/22/2022 20 ND ND 20 ND ND 20 ND ND LCS -SM 2320 B Batch: BWG1044 Date Analyzed: 07/21/2022 94.3 90-110 223 Batch: BWG1045 Date Analyzed: 07/21/2022 96.2 90 -110 227 Spk Value MRL DF 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 236 1.0 1.00 236 1.0 1.00 Page 33 of 36 Analyte QC Sample ID: BWG1099-BLKI Date Prepared: 07/22/2022 Total Dissolved Solids (TDS) QC Sample ID: BWGI099-BS1 Date Prepared: 07/22/2022 Total Dissolved Solids (TDS) QC Sample ID: BWG1099-DUP1 Date Prepared: 07/22/2022 Total Dissolved Solids (TDS) QC Sample ID: BWG1099-DUP2 Date Prepared: 07/22/2022 Total Dissolved Solids (TDS) QC Sample ID: BWG 1100-BLKl Date Prepared: 07/22/2022 Total Dissolved Solids (TDS) QC Sample ID: BWGl 100-BSl Date Prepared: 07/22/2022 Total Dissolved Solids (TDS) QC Sample ID: BWG 1100-DUPl Date Prepared: 07/22/2022 Total Dissolved Solids (TDS) QC Sample ID: BWG1100-DUP2 Date Prepared: 07/22/2022 Total Dissolved Solids (TDS) CtF WO#: 22G1743 www.ChemtechFord.com QC Report for Work Order (WO)-22G1743 % Rec RPD Limits RPD Max Result Source Cone Batch: BWG1099 Date Analyzed: 07/22/2022 ND Batch: BWG1099 Date Analyzed: 07/22/2022 102 90-110 408 Batch: BWG1099 QC Source Sample: 22G I 743-08 Date Analyzed: 07/22/2022 1 10 3860 3910 Batch: BWG1099 QC Source Sample: 22G1743-07 Date Analyzed: 07/22/2022 2 10 4140 4200 Batch: BWG 1100 Date Analyzed: 07/22/2022 ND Batch: BWG 1100 Date Analyzed: 07/22/2022 98 90 -110 392 Batch: BWGl 100 QC Source Sample: XXXXXXX-XX Date Analyzed: 07/22/2022 0 10 568 568 Batch: BWGllOO QC Source Sample: XXXXXXX-XX Date Analyzed: 07/22/2022 0 10 704 704 SpkValue MRL DF 10 1.00 400 20 1.00 20 1.00 20 1.00 10 1.00 400 20 1.00 20 1.00 20 1.00 Page 34 of 36 Surrogates Report for Work Order (WO) -22G1743 QCID Analyte BWH0006-BLK1 1,2-Dichloroethane-d4 BWH0006-BLK1 4-Bromofluorobenzene BWH0006-BLK1 Toluene-dB BWH0006-BS1 1,2-Dichloroethane-d4 BWH0006-BS1 4-Bromofluorobenzene BWH0006-BS 1 Toluene-dB BWH0006-MS1 1,2-Dichloroethane-d4 BWH0006-MS1 4-Bromofluorobenzene BWH0006-MS1 Toluene-dB BWH0006-MSD1 1,2-Dichloroethane-d4 BWH0006-MSD1 4-Bromofluorobenzene BWH0006-MSD1 Toluene-dB CtF WO#: 22G1743 www.ChemtechFord.com % Rec LCL UCL Result Blank -EPA 8260D /5030A 120 64.2 126 12.0 109 71.4 122 10.9 100 63.2 129 10.0 LCS -EPA 8260D /5030A 111 64.2 126 11.1 113 71.4 122 11.3 100 63.2 129 10.0 Matrix Spike -EPA 8260D /5030A 111 64.2 126 11.1 116 71.4 122 11.6 100 63.2 129 10.0 Matrix Spike Dup -EPA 8260D /5030A 107 64.2 126 10.7 113 71.4 122 11.3 100 63.2 129 10.0 SpkValue Batch DF 10.0 BWH0006 1.00 10.0 BWH0006 1.00 10.0 BWH0006 1.00 10.0 BWH0006 1.00 10.0 BWH0006 1.00 10.0 BWH0006 1.00 10.0 BWH0006 1.00 10.0 BWH0006 1.00 10.0 BWH0006 1.00 10.0 BWH0006 1.00 10.0 BWH0006 1.00 10.0 BWH0006 1.00 Page 35 of 36 Surrogate Recoveries (Field Samples) LabNumber Analyte 8260 Low Level Volatiles 22G1743-06 Toluene-dB 22G1743-06 4-Bromofluorobenzene 22G1743-06 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22G 17 43-07 Toluene-dB 22G1743-07 22G1743-07 4-Bromofluorobenzene 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22G 17 43-08 Toluene-dB 22G1743-08 22G1743-08 4-Bromofluorobenzene 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22G 17 43-09 Toluene-dB 22G1743-09 22G1743-09 4-Bromofluorobenzene 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22G1743-10 Toluene-dB 22G1743-10 22G1743-10 4-Bromofluorobenzene 1,2-Dichloroethane-d4 CtF WO#: 22G1743 www.ChemtechFord.com Result 10.0 11.0 11.4 10.2 11.1 11.2 10.1 11.2 11.1 10.3 10.9 11.0 10.3 11.0 11.2 Spklvl 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 %Rec 100 110 114 102 111 112 101 112 111 103 109 110 103 110 112 LCL UCL 63.2 129 71.4 122 64.2 126 63.2 129 71.4 122 64.2 126 63.2 129 71.4 122 64.2 126 63.2 129 71.4 122 64.2 126 63.2 129 71.4 122 64.2 126 Qualifier Page 36 of 36 le;l 311 Laboratories LLc a member of The GEL Group INC PO Box 30712 C�1ar1e$�On. SC 29417 2040 Savage Road Char1eston. SC 29407 P 843 556 8171 F 843.766.1178 August 22, 2022 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: White Mesa Mill GW Work Order: 587184 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on July 25, 2022. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DW16138 Enclosures Sincerely, Julie Robinson Project Manager llUIH�llllffl 1111: II IHI 1111111 gel com August 22, 2022 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843)556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 587184 ample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on July 25, 2022 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following samples: Case Narrative: Laboratory ID 587184001 587184002 587184003 587184004 587184005 587184006 587184007 587184008 587184009 587184010 587184011 587184012 587184013 Client ID MW-11 07122022 MW-31 07122022 MW-14 07132022 MW-25 07132022 MW-30 07132022 MW-36 07132022 MW-26 07142022 MW-39 07142022 MW-40_07142022 MW-24A 07192022 MW-24 07202022 MW-38 07202022 MW-65 _07202022 Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. Page 3 of 27. SDG: 587184 581\s>� Samples Shipped to: p roJect 03 Ground Water 2022 Sample ID MW-11 07122022 MW-31 07122022 MW-14 07132022 MW-25 07132022 MW-30 07132022 MW-36 07132022 MW-26 07142022 MW-39 07142022 MW-40 07142022 MW-24A 07192022 MW-24 07202022 MW-38 07202022 MW-65 _ 07202022 g c,E.,,:RGYFUELS RESOURCES Sheet 1 of 1 CHAIN OF CUSTODY GEL Laboratories, LLC Contact: Tanner Holliday -2-0-40-S-av_a_g_e_R_o_a_d________ Ph: 435 678 2221 Charleston, SC 29407 tholliday@enerqyfuels.com (843)556 8171 Chain of Custody/Sampling Analysis Request s amp ers N ame s amp1ers SI Ignature Tanner Holliday l_j(JNlt,c_�-;} Time Date Collected Collected Laboratory Analysis Requested 7/12/2022 1120 Gross Alpha 7/12/2022 1245 Gross Alpha 7/13/2022 1345 Gross Alpha 7/13/2022 1100 Gross Alpha 7/13/2022 1035 Gross Alpha 7/13/2022 1230 Gross Alpha 7/14/2022 800 Gross Alpha 7/14/2022 935 Gross Alpha 7/14/2022 1000 Gross Alpha 7/19/2022 700 Gross Alpha 7/20/2022 810 Gross Alpha 7/20/2022 830 Gross Alpha 7/20/2022 830 Gross Alpha Comments: Please send report to Kathv Weinel at kweinel@enerQyfuels.com Relinquished By:(Signature) ..:J� Page 5 of 27 SDG: 587184 Date/Time Rec ure) 7/21/202 1100 Date/Time fi]3! j Lal"ioratmies 1 LC Carrier and Tracking Number Suspecled Haznrd Information AJShi d a, a DOT Hazan.lous? B) Did the client design.11e rhe s:m,ples are lO he received ns mdioac1ivc'! C) Did the RSO clo.ssify the samples as rudioacli vc'! D) Dil1 rhc client desi •nutc sum !cs are hazardous? El Oid the RSO iJcmifr ,.t<sihk haz1llli:1? Sample Receipt Criteria Shipping co111ainers received intact and scaled? 2 Chain of custody documents included with snipmenl'/ J Samples requiring cold preservation within (0 < 6 de . C)1* 4 Daily check performed and passed on IR temperature gun? S Sample containers intact nnd scaled? 6 Samples re4uirin¥ chemical preservation at proper pH? 7 Do any samples require Volatile Analysis? 8 Samples received within holding time• 9 Sample !D's on COC match !D's on bottles• Number of conlainers received ma1d1 11 number indicated on COC? 12 Are sample conlainers idenlifiable as GEL rovided b use of GEL labels? 13 COC form is properly sii,'lled in rclin uisncd/receivcd sections? Comments (Use Continuation Form if needed): Page 6 of27 SDG: 587184 Other � .;_ >i<If Net Cuun1s > IOOcpm on samples not markeU "radiom:tive", cnntacl rhe R.idi:.uion Safoly Group fur further investi8aliun. Hazard Closs Shipped: UN#: If UN2910, ls the Radioaclil'e Shipment Survey Compliant? Yes_ No_ COC not:llion or radioactive stickers on container.; equal client designution. Maximum Net Counts Observed• (Observed Couills - Area Bnckground Couuts): �----­Classined as: Rad I Rad 2 Rad 3 COC notation or hozard labels on containers equal client designation. f Dor Eis yes, select Hazards below. PCB's Flammable Foreign Soil RCRA Asbestos Beryllium Orher: Conunents/Qualiliers (Required fur Non-Confomdng Items) Cln:Je Applicable: Sral-< bmkCn Dnmugec.l cooinincr l.r1tking con winer 01hcr (Yrscrlbf I Cilcle Arpli<nhk: Clicnr <nn1oc1cd nnll t>nn;,k,t COt" Pri:�rvnliun M�tho<l: Wet kt: kt! Pm.:k!\ O,ykc •a1t 1ernpcraturcs are recorded in Celsius Tempcrnlurc OcYk<: Serial #:.�IR�2�-�2�1 ____ _ Secondary Tempcmnm: Device Serial# (If Applicable): C""arck Arptkuhk:: S�11b: hro�cn Damaged cnru.smcr �:akm� cnn111inor 01hcr rd�.!.crihcl lf Yes. are Encores or Soil Kits present ro, �olld,f/ Ye$._ No_ NA_(lf )'cs. 1nke 10 VOA Freezer) Do littuld VOA vials contain ucid prcscrvntion? Y�-No_ NA_(lrunkmlwn. select No) i\rc lll(uid VOA vials free or headspoc.-? YcL_ No_ NA_ Su1nplc ID's anrl conlaincrs affcclcd: !D's und tests affected: I D'."l ant.I cuntuincr,,:; affected: Circle Applicable: No dates on containers No times on containers COC missing nfo Orher (describe) Circk Applicable: No container count on COC Other (tlc�trihl:J Circle Arplk11hlc: Not relinquished Orher (otescrihc) GL-CHL-SR-001 Rev 7 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 587184 Client SDG: 587184 Q3 Ground Water 2022 Project Manager: Julie Robinson Project Name: Purchase Order: DNMI00100 White Mesa Mill GW DW16138 Package Level: LEVEL3 EDD Format: EIM_DNMI GELID Client Sample ID Client Sample Desc. 587184001 MW-11_07122022 587184002 MW-31_07122022 587184003 MW-14_07132022 587184004 MW-25_07132022 587184005 MW-30_07132022 587184006 MW-36_07132022 587184007 MW-26_07142022 587184008 MW-39_07142022 587184009 MW-40_07142022 587184010 MW-24A_07192022 587184011 MW-24_07202022 Client will recollect 587184012 MW-38_07202022 587184013 MW-65_07202022 Client Sample ID Status Tests/Methods -001 MW-11_07122022 REVW GFPC, Total Alpha Radium, Liquid -002 MW-31_07122022 REVW GFPC, Total Alpha Radium, Liquid -003 MW-14_07132022 REVW GFPC, Total Alpha Radium, Liquid -004 MW-25_07132022 REVW GFPC, Total Alpha Radium, Liquid -005 MW-30_07132022 REVW GFPC, Total Alpha Radium, Liquid -006 MW-36_07132022 REVW GFPC, Total Alpha Radium, Liquid -007 MW-26_07142022 REVW GFPC, Total Alpha Radium, Liquid -008 MW-39_07142022 REVW GFPC, Total Alpha Radium, Liquid -009 MW-40_07142022 REVW GFPC, Total Alpha Radium, Liquid -010 MW-24A_07192022 REVW GFPC, Total Alpha Radium, Liquid -011 MW-24_07202022 Collect Date & Time 12-JUL-22 11:20 12-JUL-22 12:45 13-JUL-22 13:45 13-JUL-22 11:00 13-JUL-22 10:35 13-JUL-22 12:30 14-JUL-22 08:00 14-JUL-22 09:35 14-JUL-22 10:00 19-JUL-22 07:00 20-JUL-22 08:10 20-JUL-22 08:30 20-JUL-22 08:30 Product Reference Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Work Order Due Date: 22-AUG-22 Package Due Date: EDD Due Date: Due Date: JAR1 Receive Time # of Date & Time Zone Cont. 25-JUL-22 08:10 -2 25-JUL-22 08:10 -2 25-JUL-22 08:10 -2 25-JUL-22 08:10 -2 25-JUL-22 08:10 -2 25-JUL-22 08:10 -2 25-JUL-22 08:10 -2 25-JUL-22 08:10 -2 25-JUL-22 08:10 -2 25-JUL -22 08:10 -2 25-JUL-22 08:10 -2 25-JUL-22 08:10 -2 25-JUL -22 08:10 -2 Fax Date PM Comments 22-AUG-22 22-AUG-22 22-AUG-22 Lab Matrix GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER Report Date: 22-AUG-22 Work Order: 587184 Page 1 of 2 Collector: C Prelogin #: 20190487484 Project Workdef ID: 1294356 SDG Status: Closed Logged by: Fax Days to Prelog Lab Field Due Date Process CofC# 20 20 20 20 20 20 20 20 20 20 20 20 20 Aux Data Group QC QC Receive Codes s:t" 00 00 lr) tJ Cl r/.l r--­N 'I-< 0 r---11) GEL Laboratories LLC -Login Review Report -012 MW-38_07202022 -013 MW-65_07202022 REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid Product: GFCTORAL Workdef ID: 1458614 Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Gross Alpha Gross Alpha In Product Group? No Samples: 001, 002, 003, 004, 005, 006, 007, 008, 009, 010, 012, 013 Parmname Check: All parmnames scheduled properly CAS# Contingent Tests Parmname Gross Radium Alpha Action Product Name Login Requirements: Requirement Description Group Name: Group Reference: Report Date: 22-AUG-22 Work Order: 587184 Page 2 of 2 Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Client RDL or PQL & Unit Reporting Parm Included Included Custom Units Function in Sample? in QC? List? pCi/L REG y y No Samples Include? Comments Peer Review by: ____________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? _____ _ -s:t-00 - 00 lr) r--­N '+-< 0 00 ll) Julie Robinson From: Sent: Kathy Weinel <KWeinel@energyfuels.com> Monday, July 25, 2022 11 :50 AM To: Julie Robinson Subject: RE: Sample MW-24_07202022 [EXTERNAL EMAIL] Julie, Discard the sample and we will recollect ---Energy Fuels Resources (USA) Inc. Kathy Weinel Director, Regulatory Compliance From: Julie Robinson <Julie.Robinson@gel.com> Sent: Monday, July 25, 2022 8:49 AM To: Kathy Weinel <KWeinel@energyfuels.com> Cc: N. Tanner Holliday <tholliday@energyfuels.com> Subject: Sample MW-24_07202022 Good morning Kathy, Sample MW-24_072022 did not hold it nitric acid preservation. Please advise if you would like GEL to reduce the pH< 2 before proceeding with the prep and analysis. Thanks, Julie Robinson Project Manager 2040 Savage Road, Charleston, SC 29407 P.O. Box 30712. Charleston, SC 29417 Office Direct: 843.769.7393 Office Main: 843.556.8171 Fax: 843.766.1178 Disclaimer The information contained in this communication from the sender is confidential. It is intended solely for use by the recipient and others authorized to receive it. If you are not the recipient, you are hereby notified that any disclosure, copying, distribution or taking action in relation of the contents of this information is strictly prohibited and may be unlawful. This email has been scanned for viruses and malware, and may have been automatically archived by Mimecast, a leader in email security and cyber resilience. Mimecast integrates email defenses with brand protection, security awareness training, web security, compliance and other essential capabilities. Mimecast helps protect large and small organizations from malicious activity, human error and technology failure; and to lead the movement toward building a more resilient world. To find out more, visit our website. 2 Client Sample Identification Technical Information GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMIO0l Energy Fuels Resources (USA), Inc. Client SDG: 587184 GEL Work Order: 587184 The Qualifiers in this report are defined as follows: *A quality control analyte recovery is outside of specified acceptance criteria** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. Review/Validation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: j� � Date: 19 AUG 2022 Page 13 of 27 SDG: 587184 Name: Theresa Austin Title: Group Leader GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com Contact: Workorder: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Ms. Kathy Weinel 587184 QC SummarI Parmname NOM Sample _Qual QC Units Rad Gas Flow 3atch 2296158 QC120SISl296 587184001 DUP Gross Radium Alpha u 0.886 u Uncertainty +l-0.327 QC1205151299 LCS Gross Radium Alpha 1040 Uncertainty QC1205151295 MB Gross Radium Alpha u Uncertainty QC1205151297 587184001 MS Gross Radium Alpha 2150 u 0.886 Uncertainty +l-0.327 QC1205151298 587184001 MSD Gross Radium Alpha 2090 u 0.886 Uncertainty +l-0.327 Notes: Counting Uncertainty is calculated at the 68% confidence level (]-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product 0.661 pCilL +l-0.334 1000 pCi/L +I-I 1.5 0.446 pCilL +l-0.2951770 pCilL +l-21.3 1770 pCilL +l-21.3 RPO% NIA 0.0951 A B BD C D F For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low H K L M Analyte has been confirmed by GCIMS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and Jess than LLD Page 26 of 27 SDG: 587184 Reoort Date: August 19, 2022 REC% Ran e Anlst NIA JXC9 95.9 (75%-125%) 82.2 (75%-125%) 84.5 (0%-20%) Page I of Date Time 08/17122 14:4, 08/17122 14:4, 08/17122 14:4, 08/17122 14:4, 08117122 14:4, GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 -www.gel.com Workorder: 587184 Parmname M Matrix Related Failure NOM ---- NIA RPD or %Recovery limits do not apply. See case narrative QC Summary Sample Qual C Units �--- Analyte concentration is not detected above the detection limit RPO% Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification REC% Ran� Anlst NI ND NJ Q R u Ul UJ UL X y Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier h QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of Date Time NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. /\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where the duplicate value is less than 5X the RL, a control limit of +I-the RL is used to evaluate the DUP result. *Indicates that a Quality Control parameter was not within specifications.For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 27 of27 SDG: 587184 ®41 I Laboratories LLc a member of The GEL Group INC POBox8.0712 C�1arlestor1.SC29417 2040 Savage Road Charles1on. SC 29407 P 843 556.8171 F 843.7661178 August 25, 2022 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: White Mesa Mill GW Work Order: 587833 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on July 29, 2022. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DW16138 Enclosures Sincerely, �-� Julie Robinson Project Manager ll lll�Ulll�III 1111 11111111111 gel.com August 25, 2022 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843)556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 587833 ample receipt: The sample arrived at GEL Laboratories LLC, Charleston, South Carolina on July 29, 2022 for analysis. The sample was delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following sample: Case Narrative: Laboratory ID 587833001 Client ID MW-24 07282022 Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Page 3 of 13 SDG: 587833 �ID� Julie Robinson Project Manager Samples Shipped to: p roJect Q3 Ground Water 2022 Sample ID MW-24 07282022 g�� Sheet 1 of 1 &;]�r;_f E�N�ERGYFUELS RESOURCES CHAIN OF CUSTODY _G_E_L_L_a_b_o_ra_to_r_ie_s __ , L_L_C _______ Contact: Tanner Holliday 2040 Savage Road Ph: 435 678 2221 Charleston, SC 29407 tholllday@energyfuels.com (843)556 8171 Chain of Custody/Sampling Analysis Request s amp ers N ame s amp ers 1gnature Tanner Holliday I, Jr1 ArlPrc )4.//,.£1.,,,. ---- Time Date Collected Collected Laboratory Analysis Requested 7/28/2022 700 Gross Alpha Comments: Please send report to Kathv Weinel at kweinel@.energyfuels.com Page 4 of 13 SDG: 587833 Date/Time Receive 7/28/2022 1100 Date/Time 1/2-q/7,,i /d'1 Date/Time / •· Carrier and Tracking Number Suspected Ha,ard luformation A I Shi ed :is " DOT Hazardous• B) Did lhe clic::ni tlesigirnlc 1he samples arf hi he: n:.;civcd ns rndinac1ivc'! Cl Did 1hc RSO classify 1hc samples ,.s r-Jdioactive'! D) Did the c\icnl Uesi muc sam les are haz;m.Jous? El Did 1hc RSO i<lcnlifv ,ssihlc hazards? Sample Rcceipl Crilcrin Shipping co111ainers received intact and scaled? 2 Chain of custody documents included with shipment'! 3 Samples requiring cold preservation within (0 < 6 de . C)?* 4 Daily check performed and passed on IR temperature gun? 5 Sample containers intact and scnled'! 6 Samples requiring chemical preservation al proper pH? 7 Do any snmplcs require Volatile Analysis? 8 Samples received within holding time• 9 Sample !D's on COC match TD's un bollles? Number of containers received match 11 number i nJ ic.11eJ on COC? 12 Arc sample containers identiliable as GEL rovided bv use of GEL labels? 13 COC form is properly signed in relin uished/received sections? Commems (Use Conlinua1ion Funn if needed I: Page 5 of 13 SDG: 587833 SAMPLE RECEIPT & REVIEW FORM Onte Rc(civcd Courier Other � -£ ""If Net Counts> 100..:pm nn sample:,; noi mnrketl "mdiom:tive". i.:onli1L'1 lhe RitUionion S;1fc1y Grnup fur futiher invc�ti11uinn, Hazard Clnss Shipped: UN#: If UN29IO. Is lhc R:idioac1i1·• Sltipmelll Survey Compliun1? Yes_ No_ COC nntatiun nr radioactive slickers tln c�mtuiners e,1u:i.l. �licnl Jcsignation. aximum Ncl Counts Observed• (Obsen·cd Counts• Aren Bock�round Counls): CPM /mR/Hr Classified as: Rad I Rud 2 Rad 3 CDC nolnlion or hnzard labels on containers equal cliclll designation. f Dor Eis yes, selccl l·farnrds below. PC B's Flnmnrnble Foreign Soil RCRA Asheslos Beryllium 01her: Cnmmcnls/Qualificrs (Required rur Non-Conforming ltcmsJ Cir�le Applic:1bl"; Seals broken Dam.agcc.J c,,n1ai11cr Leuking contuii1cr Other (Jcs1.:ribcJ Circle Applicable: Clicnl contacted ilnd provided COC Presl!rvatiun McthuJ: Wei h:e kt: Packs *all lempenllures arc recun..lcd in Celsius Temperature Device Serial #:.�IR�2�·�2�1 ____ _ Secondary Temperature Device Serini N (If Applicable): coc Cl'C(IIC'd 11110n rccl'ipt. CU'clc Applkahlc: Sculs hrokcn Damug.cd cnn1aincr Leaking container Other (dcscrihcl S.lmplc IO's nnd Containers AITcclcd: fl PrcserY-Jlion aJJcc.J. l..ut#: r Yes, nre Encores or Soil Kiis present ror solidi? Yes_ No_ NA_(lf yes, take lo VOA Freezer) Do liquid VOA vials contain acid preservation'/ Yes_ No_ NA_(lfunknown, select Nol Are liquid VOA vials free ofheadspnce? Yes_ No_ NA_ Sampll! ID'!li und containers :.iITcclcd: ID's and ICSls affected: I D's umJ cuntaimm; affected: Circle Applicable: No dales on conlainers No lime., on co111ainc1� COC missing info 01her (d<scribe) Circle Applicable: No conlniner coulll on COC 01hcr (dc�cribcJ Circle Applicable: Nol rclin�uished 01hcr (liescrihe) GL·CHL·SR·001 Rev 7 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 587833 Client SDG: 587833 Q3 Ground Water 2022 Work Order Due Date: 26-AUG-22 Report Date: 25-AUG-22 Work Order: 587833 Page 1 of 2 Collector: C Project Manager: Project Name: Purchase Order: Package Level: EDD Format: Julie Robinson DNMI00100 White Mesa Mill GW DW16138 LEVEL3 EIM_DNMI GELID Client Sample ID Client Sample Desc. 587833001 MW-24_07282022 Client Sample ID -001 MW-24_07282022 Status Tests/Methods REVW GFPC, Total Alpha Radium, Liquid Collect Date & Time Package Due Date: EDD Due Date: Due Date: JAR1 Receive Time # of Date & Time Zone Cont. 28-JUL-22 07:00 29-JUL-22 10:45 -2 Product Reference Gross Alpha Fax Date PM Comments Product: GFCTORAL Workdef ID: 1458614 In Product Group? No Group Name: Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Samples: 001 Parmname Check: All parmnames scheduled properly CAS# Parmname Gross Radium Alpha Action Product Name Contingent Tests Login Requirements: Description Client RDL or PQL & Unit Samples 26-AUG-22 26-AUG-22 26-AUG-22 Prelogin #: 20190487484 Project Workdef ID: 1294356 SDG Status: Closed Logged by: Lab Matrix Fax Days to Due Date Process CofC # Prelog Lab Field Group QC QC GROUND WATER 20 Aux Data Group Reference: Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Reporting Parm Included Included Custom Units Function in Sample? in QC? List? pCi/L REG y y No Receive Codes M M 00 c---00 l(") 0 Q rJJ _R _e....;q _ui _re_m_en_t _____________________ ln_c_lu_d_e_?_C_om_m_e_n _ts _________________________ �M GEL Laboratories LLC -Login Review Report Peer Review by: __________ _ Work Order (SDG#), PO# Checked? ____ _ Report Date: 25-AUG-22 Work Order: 587833 Page 2 of 2 C of C signed in receiver location? ____ _ M M 00 r:---00 l/) ci 0 r/J. M ...... 4-, 0 r--­ (!) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMIO0I Energy Fuels Resources (USA), Inc. Client SDG: 587833 GEL Work Order: 587833 The Qualifiers in this report are defined as follows: *A quality control analyte recovery is outside of specified acceptance criteria** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. Review/Validation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: j� � Date: 24 AUG 2022 Page 10 of 13 SDG: 587833 Name: Theresa Austin Title: Group Leader GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Contact: Lakewood, Colorado Ms. Kathy Weinel Workorder: 587833 Parmname ---- Rad Gas Flow 3atch 2300524 QC1205159247 587833001 DUP Gross Radium Alpha QC1205159250 LCS Gross Radium Alpha QC I 205159246 MB Gross Radium Alpha QC1205159248 587833001 Gross Radium Alpha QC 1205 I 59249 587833001 Gross Radium Alpha Notes: MS MSD NOM Uncertainty 539 Uncertainty Uncertainty 2150 Uncertainty 2110 Uncertainty Sam le Qu_a_l --�C 2.55 +/-0.449 2.55 +/-0.449 2.55 +/-0.449 u 2.85 +/-0.475 410 +/-5.10 0.340 +/-0.234 1640 +/-16.4 1610 +/-21.1 Counting Uncertainty is calculated at the 68% confidence level (I-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product Units pCi/L pCi/L pCi/L pCi/L pCi/L 11.2 2.21 A B BD C D F H K L M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Page 12 of 13 SDG: 587833 Reoort Date: August 24, 2022 Page I of Range Anlst Date Time (0% -100%) JXC9 08/19/22 11 :3 76 (75%-125%) 08/22/22 12: J. 08/19/22 11 :3 76.3 (75%-125%) 08/22/22 12:1- 76.1 (0%-20%) 08/19/22 11 :3 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 -www.gel.com Workorder: Parm name ----- 587833 M Matrix Related Failure NOM NIA RPD or %Recovery limits do not apply. See case narrative QC Summary Sample Qual Q_C Units Analyte concentration is not detected above the detection limit RPO% Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification REC% Range Anlst NI ND NJ Q R u UI UJ UL X y Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier (\ h QC Samples were not spiked with this compound RPO of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of Date Time NI A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. /\ The Relative Percent Oil'� rcnce (RPO) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where the duplicate value is less than 5X the RL, a control limit of +I-the RL is used to evaluate the DUP result. *Indicates that a Quality Control parameter was not within specifications.For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 13 of 13 SDG: 587833 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA8ORI\T0RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-11_08082022 Matrix: Water Date Sampled: 8/8/22 12:45 lnnr!,!anit· Chloride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) Manganese, Dissolved Result 67.4 2.45 1260 3230 0.201 Project Name: August Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 1.0 0.100 20.0 20 0.0100 PO#: Receipt: 8/11/22 11:20@ -0.3 °C Date Reported: 9/1/2022 Project Name: August Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 CtF WO#: 22H1255 Preparation Date/Time 8/16/22 8/16/22 8/30/22 8/12/22 8/19/22 Lab ID: 22H1255-01 Analysis Date/Time 8/17/22 8/16/22 8/31/22 8/12/22 8/19/22 Page 3 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA8OR,H0 llt ES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-25_08092022 Matrix: Water Date Sampled: 8/9/22 11 :05 lnorcanit· Total Dissolved Solids (TDS) Result 2780 Project Name: August Ground Water 2022 www.ChemtechFord.com Units mg/L Certificate of Analysis Minimum Reporting Limit 20 PO#: Receipt: 8/11/22 11 :20@ -0.3 °C Date Reported: 9/1/2022 Project Name: August Ground Water 2022 Sampled By: Tanner Holliday Method SM2540C CtF WO#: 22H1255 Preparation Date/Time 8/12/22 Lab ID: 22H1255-02 Analysis Date/Time 8/12/22 fuJilll Page 4 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA8O1P,T0IIIE5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-26_08092022 Matrix: Water Date Sampled: 8/9/22 13:00 lnurcanil Chloride Nitrate+ Nitrite, Total, as N Total Dissolved Solids (TDS) \ olatik Organ ii' ( om po 111111, Chloroform 65.0 1.56 3120 1120 Project Name: August Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L ug/L Certificate of Analysis Minimum Reporting Limit 1.0 0.100 20 100 PO#: Receipt: 8/11/22 11 :20@ -0.3 °C Date Reported: 9/1/2022 Project Name: August Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 SM2540C EPA 82600 /5030A CtF WO#: 22H1255 Preparation Date/Time 8/19/22 8/16/22 8/12/22 8/12/22 Lab ID: 22H1255-03 Analysis Date/Time 8/19/22 8/16/22 8/12/22 8/12/22 Fla2(s) Page 5 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l/\80'<,\TOAIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-30_08092022 Matrix: Water Date Sampled: 8/9/22 10:50 lnorl!allil Chloride Nitrate+ Nitrite, Total, as N Total Dissolved Solids (TDS) Selenium, Dissolved Uranium, Dissolved Result 185 13.5 1580 0.0643 0.0101 Project Name: August Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 100 0.500 20 0.0050 0.0003 PO#: Receipt: 8/11/22 11:20@ -0.3 ·c Date Reported: 9/1/2022 Project Name: August Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 SM 2540 C EPA200.8 EPA200.8 CtF WO#: 22H1255 Preparation Date/Time 8/19/22 8/16/22 8/12/22 8/19/22 8/19/22 Lab ID: 22H1255-04 Analysis Date/Time 8/19/22 8/17/22 8/12/22 8/19/22 8/19/22 � Page 6 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH•FORD Serving the lntermountain West Since 1953 lASOR;.TORlf:S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-31_08082022 Matrix: Water Date Sampled: 8/8/22 13:40 lnoq,:arm Chloride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \kta1' Uranium, Dissolved Result 396 16.8 1230 2700 0.0227 Project Name: August Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 1.0 0.500 20.0 20 0.0003 PO#: Receipt: 8/11/22 11:20@ -0.3 °C Date Reported: 9/1/2022 Project Name: August Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 EPA300.0 SM 2540 C EPA200.8 CtF WO#: 22H1255 Preparation Date/Time 8/16/22 8/16/22 8/30/22 8/12/22 8/19/22 Lab ID: 22H1255-05 Analysis Date/Time 8/17/22 8/17/22 8/31/22 8/12/22 8/19/22 .E!JWfil Page 7 of 20 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA60RATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-65_08092022 Matrix: Water Date Sampled: 8/9/22 10:50 lrwrcanil Chloride Nitrate+ Nitrite, Total, as N Total Dissolved Solids (TDS) Selenium, Dissolved Uranium, Dissolved Result 180 16.1 1700 0.0638 0.0100 Project Name: August Ground Water 2022 www. Chem tech Ford. com Units mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 100 0.500 20 0.0050 0.0003 PO#: Receipt: 8/11/22 11:20@ -0.3 °C Date Reported: 9/1/2022 Project Name: August Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 SM 2540 C EPA 200.8 EPA 200.8 CtF WO#: 22H1255 Preparation Date/Time 8/19/22 8/16/22 8/12/22 8/19/22 8/19/22 Lab ID: 22H1255-06 Analysis Date/Time 8/20/22 8/17/22 8/12/22 8/19/22 8/19/22 Flag(s) Page 8 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA6ORAT0AIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 8/9/22 13:00 \ olal1h· ( )r:!allll' ( '11111p11111ul, Chloroform < 1.0 Project Name: August Ground Water 2022 www.ChemtechFord.com Units ug/L Certificate of Analysis Minimum Reporting Limit 1.0 PO#: Receipt: 8/11/22 11:20@ -0.3 °C Date Reported: 9/1/2022 Project Name: August Ground Water 2022 Sampled By: Tanner Holliday Method EPA 8260D /5030A CtF WO#: 22H1255 Preparation Date/Time 8/12/22 Lab ID: 22H1255-07 Analysis Date/Time 8/12/22 Page 9 of 20 Client Service Contact: 801.262. 7299 SeNing the lntermountain West since 1953 Page 1 of 20 Energy Fuels Resources, Inc. Project: August Ground Water 2022 Project Manager: Tanner Holliday Laboratory ID 22H1255-01 22H1255-02 22H1255-03 22H1255-04 22H1255-05 22H1255-06 22H1255-07 Sample Name MW-11_08082022 MW-25_08092022 MW-26_08092022 MW-30_08092022 MW-31_08082022 MW-65_08092022 Trip Blank Work Order Report Narrative Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions There are no corrective actions associated with this work order. Project Name: August Ground Water 2022 www.ChemtechFord.com CtF WO#: 22H1255 Page 2 of 20 CHEMTECH·FORD Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Certificate of Analysis Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Abbreviations PO#: Receipt: 8/11/22 11:20@ -0.3 °C Date Reported: 9/1/2022 Project Name: August Ground Water 2022 Project Name: August Ground Water 2022 www.ChemtechFord.com CtF WO#: 22H1255 Page 10 of 20 1 � Client: Address: Contact: Phone#: Email: Project Name: Project#: PO#: Sampler Name: American West Analytical Laboratories 463 w. 3600 s san Lake City, ITT 84115 Phone# (801) 263--'!686 Toll Free# (888) 263--'!686 Fax# (801) 263--'!687 Email awal@awal�abs.com www.awal-labs.com Energy Fuels Resources, Inc. 6425 S. Hwy. 191 Blanding, UT 84511 Tlllll1er Holliday (435) 678-2221 Cell#: thoWday@;-ergyfueJs.com; kwe1Del@ellerafaels.com; August Ground Water 2022 Tanner Holliday )JH\�5 Date Samele ID: Samoled 1 IIW-11_08082022 2 JIW-25_08092022 3 IIW-26_08092022 • IIW-30_08092022 s BW-31_08082022 6 BW-65_08092022 7 8 9 Trip Blank 0 , 2 : IRollnq<Jiohod by--1 �1,, .. u•tunt ' � - - · • Jl.✓J,LdV "llnlN""'°' ToMG<Ho�ldnv R�by: '.� ......... Pr!ntNomo: Rellnqulshod by: !:innetu,e P!intNams: Relinquished by: Slnnature ..__. __ 8/8/2022 8/9/2022 8/9/2022 8/9/2022 8/8/2022 8/9/2022 8/9/2022 Oolo: 811()(.! T,mo: t,,.. Do.to Tlmo Oate: Time: Date: Time: V � .:J 1 z 187 y 4Y 03 9595 0282 / CHAIN OF CUSTODY 22'/ltzss All analysis will be conducted using NELAP accrediled methods and all data will be reported using AWA.L's slandard analyte ltSb and reporting limits: (POL) unlese specifically requested otherwise on this Chain of Custody and/or attached documentation AWAL Lab sample Set# Page of 1 I QC Level: I Turn Around Time: Unless other am1ngements have been made. Due Date: signed repona w4II be emailed by 5:00 pm on 3 Standard the day lhey an!I due X Include EDD: Laboratory Use Only LOCUS UPLOAD EXCBJ. SampleoWen, X Field Fillered For: l>iaaolved Metals , Shipped« hand-...S co cij' 0 co 00 00 0 2 AmbiMtO<� 0 .3 0 0 0 0 For Compliance With: "' 0 0 0 ......0 "'"' ;:::-D NELAP 3 Tempen,ture ·cr--"' ;:::-;:::-----0 ---0 ci' D RCRA 0 r--0 c:i 0 D CWA •Received Brokonlleaklrlg 0 0 £:!. 0 0 I::!. I() D SOWA 0 I::!. I::!. "' (lmpn>p911y Sealed) 0 £:!. 0 • ] •� D ELAP/A2LA y N 9 9 0 0 D NLLAP 5 0 !0 e � II 0 'ii a 'ii 0 D Non-Compliance 5 f'l-1YP,_.,ed 5 0 I! 1 0 5 "l .s D Other: y J ... 0 C-edatl>Mch � � II .. (J i::i u II 0 0 0 0 .2 y N C :s Cl) "II "II "II "II "II 0 ffl �0 0 0 ..,. 0 0 0 1 "' :r; � � "' � � 1 :!. u Known Hazards 6 Received Wihn .. -0 :!. � ! 0 i "Holding limeo Time (.) Q.N : ID :• E 0 6 Q i 0 y Samoled .. � II: Q .. Q iS iS Q >Samele Comments 1245 4 w X X X X X 1105 I w X 1300 6 w X X X X ,-onOulorP� y N NA 1050 4 w X X X X X 2 Unbroken on Ou1or P� 1340 4 w X X X X X y N NA 1050 X X X X X 3 P.-onS....,,.., 4 w y N NA •Unl>r""8nanS...., 1300 3 w X y N NA -.s...., � and COC Reconl7 y N Reoe;ved by: Date: Special Instructions: Time: IPri!,t Name: , Sample containers for metals were field filtered. See the R""""'ed. V ,; d-/4., ✓ D•�f,7z z....-Analytical Scope of Work for Reporting Limits and voe analyte 5""'••-_! j _,,,_ ./ ' Tlrne:/ / 2( '\ list. Print Ne.me: Reoeived by: Date: Siana11J19 ,lime: f>ri.nlNeme: Rooetved by: pale: 5 ..... 1un1 Page 11 of 2 '""''" Print Name: 0 I Work Order # 2 '7 !-I / 2 "S" 'S ---------------"------- \ Delivery Method: '-g UPS D USPS F dE D e X D Ch emtec hC ouner o Walk-in D Customer Courier -�Cherntech Lot# Sample# Container Preservative 0 \,O",�il Af A \/Jf\ \,.. 'M tt�.£ Y1. 1 'Z,.\b A/, r O'L. f-\kzf 63 A'f? AWI\L n l i.1 bA'te \,rJ (3) l'L03 07 \.Jc� 1 A \,\]Al i!:" t j� l! i:a � "i C 11 ei s :, "' 1; .5 1; .., ' i .. i! E j j J!. 1! .t 3! '1 Misc J Volume .. (oz/ml) i'i! CHEMTECH FORD LABORATORIES Sample Receipt Receiving Temperature oc G 3 -· Comments T\'\� 12.hnK CHEMTECH-FORD LABOR/\T�;P1t:S Sample Condition (check if yes I ITcustody Seals Containers Intact COC can be matched to bottles Received on Ice Correct Container;(s} Sutricent Sample Volume Received within Holding Time Plastic Containers A,. Pta11tc Unpn�set\l� 8- Miscellaneous Plastic C• Cyan;de Qt (NaOH) [- Coliform/Ecoli/HPC F• Sulfide Qt (Zn Acetate) l• Mercurv 1631 M• Metals p;nl (HN03) N• Nutrient P;nt (H2S04) R· Rad;ologkal (HN03) S-Sludge Cups/rubs Q� Plastic Bag Glass Containers D- 625 (Na25203) G-Glass Unpreserved H- HAAs (NH4CII J-508/515/525 (Na2S03) K· 515.3 Herbicides 0-OH & Grease (HCI) P- Phenols (H2S04) T- TOC/rOX (H3P04) U· 531 (MCAA, Na25203) V· 524/rHMs (Ascorbk Ac;d) W- 8260 voe (1:1 HCI) X-Vial Unpreserved Y-624/504 (Na25203) z. Miscellaneous Glass Page 12 of 20 Analyte QC Sample ID: BWHI 180-BLKl Date Prepared: 08/19/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWHI 180-BS l Date Prepared: 08/19/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWHI 180-MSJ Date Prepared: 08/19/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWHI180-MS2 Date Prepared: 08/19/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWHl I 80-MS3 Date Prepared: 08/19/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved CtF WO#: 22H1255 www.ChemtechFord.com QC Report for Work Order (WO) -22H1255 %Rec RPO Limits RPO Max Result Source Cone Blank -EPA 200.8 Batch: BWHI 180 Date Analyzed: 08/19/2022 ND ND ND LCS -EPA 200.8 Batch: BWHl 180 Date Analyzed: 08/19/2022 98.9 85 -115 0.040 102 85 -115 0.041 107 85 -115 0.043 Matrix Spike -EPA 200.8 Batch: BWH1180 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/19/2022 93.5 70 -130 0.049 0.012 107 70 -130 0.046 0.003 104 70 -130 0.048 0.007 Batch: BWH1180 QC Source Sample: 22Hl 255-04 Date Analyzed: 08/19/2022 94.6 70 -130 0.045 0.007 100 70 -130 0.104 0.064 105 70 -130 0.052 0.010 Batch: BWHl 180 QC Source Sample: 22HI 255-06 Date Analyzed: 08/19/2022 94.3 70 -130 0.045 0.008 99.9 70 -130 0.104 0.064 106 70 -130 0.052 0.010 Spk Value MRL OF 0.0100 1.00 0.0050 1.00 0.0003 1.00 0.0400 0.0005 1.00 0.0400 0.0005 1.00 0.0400 0.0003 1.00 0.0400 0.0005 1.00 0.0400 0.0005 1.00 0.0400 0.0003 1.00 0.0400 0.0005 1.00 0.0400 0.0005 1.00 0.0400 0.0003 1.00 0.0400 0.0005 1.00 0.0400 0.0005 1.00 0.0400 0.0003 1.00 Page 13 of 20 Analyte QC Sample ID: BWH0933-BLK1 Date Prepared: 08/16/2022 Chloride QC Sample ID: BWHI 196-BLKI Date Prepared: 08/19/2022 Chloride QC Sample ID: BWHl 197-BLKl Date Prepared: 08/19/2022 Chloride QC Sample ID: BWH1777-BLKI Date Prepared: 08/30/2022 Sulfate QC Sample ID: BWH0933-BS I Date Prepared: 08/16/2022 Chloride QC Sample ID: BWHl 196-BSl Date Prepared: 08/19/2022 Chloride QC Sample ID: BWHl 197-BSl Date Prepared: 08/19/2022 Chloride QC Sample ID: BWH1777-BSI Date Prepared: 08/30/2022 Sulfate QC Sample ID: BWH0933-MS I Date Prepared: 08/16/2022 Chloride QC Sample ID: BWH0933-MS2 Date Prepared: 08/16/2022 Chloride QC Sample ID: BWHl 196-MSI Date Prepared: 08/19/2022 Chloride QC Sample ID: BWHl l 96-MS2 Date Prepared: 08/19/2022 Chloride QC Sample ID: BWHl 197-MSl Date Prepared: 08/19/2022 Chloride QC Sample ID: BWHl 197-MS2 Date Prepared: 08/19/2022 Chloride CtF WO#: 22H1255 www. Chem tech Ford. com QC Report for Work Order (WO) -22H1255 % Rec RPD Limits RPD Max Result Source Cone Blank -EPA 300.0 Batch: BWH0933 Date Analyzed: 08/l 7 /2022 ND Batch: BWHl 196 Date Analyzed: 08/19/2022 ND Batch: BWH1197 Date Analyzed: 08/20/2022 ND Batch: BWH1777 Date Analyzed: 08/31/2022 ND LCS - EPA 300.0 Batch: BWH0933 Date Analyzed: 08/17/2022 102 90 - 110 50.9 Batch: BWHl 196 Date Analyzed: 08/19/2022 101 90 -110 50.7 Batch: BWHI 197 Date Analyzed: 08/20/2022 102 90 -110 50.8 Batch: BWH1777 Date Analyzed: 08/3 l /2022 98.7 90 -110 49.3 Matrix Spike - EPA 300.0 Batch: BWH0933 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/17/2022 103 80 -120 12.7 1.2 Batch: BWH0933 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/17/2022 103 80 -120 16.3 4.9 Batch: BWHl 196 QC Source Sample: 22Hl255-03 Date Analyzed: 08/19/2022 102 80 -120 1080 65.0 Batch: BWHl 196 QC Source Sample: 22Hl255-04 Date Analyzed: 08/19/2022 103 80 -120 1210 185 Batch: BWHl 197 QC Source Sample: 22H1255-06 Date Analyzed: 08/20/2022 99.2 80 -120 1170 180 Batch: B WHl 197 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/20/2022 101 80 -120 16.9 5.7 Spk Value MRL DF 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 50.0 1.0 1.00 50.0 1.0 1.00 50.0 1.0 1.00 50.0 1.0 1.00 11.1 1.1 1.00 11.1 1.1 1.00 1000 110 1.00 1000 110 1.00 1000 110 1.00 11.1 1.1 1.00 Page 14 of 20 Analyte QC Sample ID: BWH1777-MS1 Date Prepared: 08/30/2022 Sulfate QC Sample ID: BWHl777-MS2 Date Prepared: 08/30/2022 Sulfate QC Sample ID: BWH0933-MSD l Date Prepared: 08/16/2022 Chloride QC Sample ID: BWH0933-MSD2 Date Prepared: 08/16/2022 Chloride QC Sample ID: BWH1196-MSDI Date Prepared: 08/19/2022 Chloride QC Sample ID: BWHl l 96-MSD2 Date Prepared: 08/19/2022 Chloride QC Sample ID: BWHI 197-MSDI Date Prepared: 08/19/2022 Chloride QC Sample ID: BWH1197-MSD2 Date Prepared: 08/19/2022 Chloride QC Sample ID: BWHI 777-MSDl Date Prepared: 08/30/2022 Sulfate QC Sample ID: BWH l 777-MSD2 Date Prepared: 08/30/2022 Sulfate CtF WO#: 22H1255 www.ChemtechFord.com QC Report for Work Order (WO) -22H1255 %Rec RPD Limits RPD Max Result Source Cone Matrix Spike -EPA 300.0 (cont.) Batch: BWH1777 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/31/2022 97.2 80 -120 139 42.0 Batch: BWHl 777 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/31/2022 104 80 -120 66.3 54.7 Matrix Spike Dup -EPA 300.0 Batch: BWH0933 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/17/2022 104 0.913 80 -120 20 12.8 1.2 Batch: BWH0933 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/17/2022 105 1.64 80 -120 20 16.6 4.9 Batch: BWHl 196 QC Source Sample: 22Hl255-03 Date Analyzed: 08/19/2022 99.7 1.69 80 - 120 20 1060 65.0 Batch: BWHI 196 QC Source Sample: 22Hl255-04 Date Analyzed: 08/19/2022 102 0.699 80 -120 20 1210 185 Batch: BWHl 197 QC Source Sample: 22H1255-06 Date Analyzed: 08/20/2022 101 1.34 80 -120 20 1190 180 Batch: BWHI 197 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/20/2022 103 1.58 80 -120 20 17.2 5.7 Batch: BWHl 777 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/31/2022 96.0 0.906 80 -120 20 138 42.0 Batch: BWI-11777 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/31/2022 105 0.132 80 -120 20 66.4 54.7 Spk Value MRL DF 100 11.0 1.00 11.1 1.1 1.00 11.1 1.1 1.00 11.1 1.1 1.00 1000 110 1.00 1000 110 1.00 1000 110 1.00 11.1 1.1 1.00 100 11.0 1.00 11.1 1.1 1.00 Page 15 of20 Analyte QC Sample ID: BWH0908-BLKI Date Prepared: 08/16/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWH0908-BSI Date Prepared: 08/16/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWH0908-MS1 Date Prepared: 08/16/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWH0908-MS2 Date Prepared: 08/16/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWH0908-MS3 Date Prepared: 08/16/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWH0908-MS4 Date Prepared: 08/16/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWH0908-MSD1 Date Prepared: 08/16/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWH0908-MSD2 Date Prepared: 08/16/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWH0908-MSD3 Date Prepared: 08/16/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWH0908-MSD4 Date Prepared: 08/16/2022 Nitrate + Nitrite, Total, as N CtF WO#: 22H1255 www.ChemtechFord.com QC Report for Work Order (WO) -22H1255 % Rec RPO Limits RPO Max Result Source Cone Blank -EPA 353.2 Batch: BWH0908 Date Analyzed: 08/16/2022 ND LCS -EPA 353.2 Batch: BWH0908 Date Analyzed: 08/16/2022 93.8 80 -120 1.88 Matrix Spike -EPA 353.2 Batch: BWH0908 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/16/2022 98.1 80 -120 1.40 0.424 Batch: BWH0908 QC Source Sample: 22HI 255-03 Date Analyzed: 08/16/2022 99.0 80 -120 2.56 1.56 Batch: BWH0908 QC Source Sample: 22HI 255-04 Date Analyzed: 08/17/2022 102 80-120 14.6 13.5 Batch: BWH0908 QC Source Sample: 22Hl255-06 Date Analyzed: 08/17/2022 102 80 -120 17.1 16.1 Matrix Spike Dup -EPA 353.2 Batch: BWH0908 QC Source Sample: XXXXXXX-XX Date Analyzed: 08/16/2022 88.2 7.30 80 -120 20 1.31 0.424 Batch: BWH0908 QC Source Sample: 22H 1255-03 Date Analyzed: 08/16/2022 116 6.62 80 -120 20 2.73 1.56 Batch: BWH0908 QC Source Sample: 22H1255-04 Date Analyzed: 08/17/2022 103 0.0618 80 -120 20 14.6 13.5 Batch: BWH0908 QC Source Sample: 22H 1255-06 Date Analyzed: 08/17/2022 84.3 1.06 80 -120 20 16.9 16.1 Spk Value MRL OF 0.100 1.00 2.00 0.100 1.00 1.00 0.100 1.00 1.00 0.100 1.00 1.00 0.500 5.00 1.00 0.500 5.00 1.00 0.100 1.00 1.00 0.100 1.00 1.00 0.500 5.00 1.00 0.500 5.00 Page 16 of 20 QC Report for Work Order (WO) -22H1255 Analyte % Rec RPO Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 8260D /5030A QC Sample ID: BWH081 l-BLKI Batch: BWH081 l Date Prepared: 08/12/2022 Date Analyzed: 08/12/2022 Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chlorornethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetra hyd rofu ran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 LCS -EPA 8260D /5030A QC Sample ID: BWH08I l-BS1 Batch: BWH08I l Date Prepared: 08/12/2022 Date Analyzed: 08/12/2022 Acetone 112 70 -130 112 100 10.0 1.00 Benzene 106 70 -130 10.6 10.0 1.0 1.00 Carbon Tetrachloride 103 70 -130 10.3 10.0 1.0 1.00 Chloroform 112 70 -130 11.2 10.0 1.0 1.00 Chloromethane 103 70 -130 10.3 10.0 1.0 1.00 Methyl Ethyl Ketone 111 70 -130 111 100 10.0 1.00 Methylene Chloride 115 70 -130 11.5 10.0 1.0 1.00 Naphthalene 103 70 -130 10.3 10.0 1.0 1.00 Tetrahydrofuran 108 70 - 130 10.8 10.0 1.0 1.00 Toluene 104 70 -130 10.4 10.0 1.0 1.00 Xylenes, total 106 70 -130 31.9 30.0 1.0 1.00 Matrix Spike -EPA 8260D /5030A QC Sample ID: BWH08ll-MS1 Batch: BWH081 l QC Source Sample: 22Hl255-03 Date Prepared: 08/12/2022 Date Analyzed: 08/12/2022 Acetone 116 70 -130 578 ND 500 50.0 1.00 Benzene 79.3 70-130 39.6 ND 50.0 5.0 1.00 Carbon Tetrachloride 52.2 70 -130 26.1 ND 50.0 5.0 1.00 MS-Low -Estimated low due to Matrix Spike recovery. Chloroform -112 70 -130 1070 1120 50.0 5.0 1.00 MS-High -Estimated high due to Matrix Spike recovery. Chlorornethane 64.9 70 -130 32.4 ND 50.0 5.0 1.00 MS-Low -Estimated low due to Matrix Spike recovery. Methyl Ethyl Ketone 108 70 -130 541 ND 500 50.0 1.00 Methylene Chloride 95.7 70 -130 47.8 ND 50.0 5.0 1.00 Naphthalene 99.7 70-130 49.8 ND 50.0 5.0 1.00 Tetrahydrofuran 103 70 -130 51.6 ND 50.0 5.0 1.00 Toluene 76.4 70 -130 38.2 ND 50.0 5.0 1.00 Xylenes, total 77.8 70 -130 117 ND 150 5.0 1.00 Matrix Spike Dup -EPA 8260D /5030A QC Sample ID: BWH081 l-MSD1 Batch: BWH0811 QC Source Sample: 22Hl255-03 Date Prepared: 08/12/2022 Date Analyzed: 08/12/2022 Acetone 116 0.673 70 -130 20 581 ND 500 50.0 1.00 Benzene 74.4 6.38 70 -130 20 37.2 ND 50.0 5.0 1.00 Carbon Tetrachloride 50.3 3.71 70-130 20 25.2 ND 50.0 5.0 1.00 MS-Low -Estimated low due to Matrix Spike recovery. CtF WO#: 22H1255 www.ChemtechFord.com Page 17 of 20 QC Report for Work Order (WO) -22H1255 Analyte %Rec RPD Limits RPD Max Result Source Cone Matrix Spike Dup - EPA 82600 /5030A (cont.) QC Sample ID: BWH0811-MSD1 Batch: BWH0811 QC Source Sample: 22Hl255-03 Date Prepared: 08/12/2022 Date Analyzed: 08/12/2022 Chloroform -164 -38.1 MS-High -Estimated high due to Matrix Spike recovery. Chloromethane 63.3 2.50 MS-Low -Estimated low due to Matrix Spike recovery. Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total CtF WO#: 22H1255 www.ChemtechFord.com 106 2.12 93.5 2.33 97.2 2.54 108 4.17 72.0 5.93 75.1 3.62 70 -130 70 -130 70 -130 70 -130 70 -130 70 -130 70 -130 70 -130 20 1040 1120 20 31.6 ND 20 530 ND 20 46.8 ND 20 48.6 ND 20 53.8 ND 20 36.0 ND 20 113 ND Spk Value MRL DF 50.0 5.0 1.00 50.0 5.0 1.00 500 50.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 150 5.0 1.00 Page 18 of20 Analyte QC Sample ID: BWH0740-BLKI Date Prepared: 08/12/2022 Total Dissolved Solids (TDS) QC Sample ID: BWH0741-BLKI Date Prepared: 08/12/2022 Total Dissolved Solids (TDS) QC Sample ID: BWH0740-DUP1 Date Prepared: 08/12/2022 Total Dissolved Solids (TDS) QC Sample ID: BWH0740-DUP2 Date Prepared: 08/12/2022 Total Dissolved Solids (TDS) QC Sample ID: BWH0741-DUP1 Date Prepared: 08/12/2022 Total Dissolved Solids (TDS) QC Sample ID: BWH0741-DUP2 Date Prepared: 08/12/2022 Total Dissolved Solids (TDS) QC Sample ID: BWH0740-BSI Date Prepared: 08/12/2022 Total Dissolved Solids (TDS) QC Sample ID: BWH0741-BS1 Date Prepared: 08/12/2022 Total Dissolved Solids (TDS) C!F WO#: 22H1255 www.ChemtechFord.com QC Report for Work Order (WO) -22H1255 %Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Blank -SM 2540 C Batch: BWH0740 Date Analyzed: 08/12/2022 ND 10 1.00 Batch: BWH074 l Date Analyzed: 08/12/2022 ND 10 1.00 Duplicate - SM 2540 C Batch: BWH0740 QC Source Sample: 22Hl255-04 Date Analyzed: 08/12/2022 10 10 1420 1580 20 1.00 Batch: BWH0740 QC Source Sample: 22Hl255-06 Date Analyzed: 08/12/2022 10 10 1540 1700 20 1.00 Batch: BWH0741 QC Source Sample: 22Hl 255-03 Date Analyzed: 08/12/2022 1 10 3090 3120 20 1.00 Batch: BWH074I QC Source Sample: XXXXXXX-XX Date Analyzed: 08/12/2022 0 10 376 376 20 1.00 LCS -SM 2540 C Batch: BWH0740 Date Analyzed: 08/12/2022 93 90 -110 372 400 20 1.00 Batch: BWH074 l Date Analyzed: 08/12/2022 95 90 -110 380 400 20 1.00 Page 19 of 20 Surrogates Report for Work Order (WO) -22H1255 QCID Analyte %Rec LCL UCL Result Spk Value Blank -EPA 8260D /5030A BWH0B11-BLK1 1,2-Dichloroethane-d4 110 64.2 126 11.0 10.0 BWH0811-BLK1 4-Bromofluorobenzene 103 71.4 125 10.3 10.0 BWH0B11-BLK1 Toluene-dB 100 63.2 129 10.0 10.0 LCS -EPA 8260D /5030A BWH0811-BS1 1,2-Dichloroethane-d4 99.4 64.2 126 9.94 10.0 BWH0B11-BS1 4-Bromofluorobenzene 104 71.4 125 10.4 10.0 BWH0811-BS1 Toluene-dB 99.6 63.2 129 9.96 10.0 Matrix Spike -EPA 8260D /5030A BWH0811-MS1 1,2-Dichloroethane-d4 104 64.2 126 52.1 50.0 BWH0811-MS1 4-Bromofluorobenzene 102 71.4 125 51.2 50.0 BWH0811-MS1 Toluene-dB 100 63.2 129 50.0 50.0 Matrix Spike Dup -EPA 8260D /5030A BWH0811-MSD1 1,2-Dichloroethane-d4 102 64.2 126 51.2 50.0 BWH0B11-MSD1 4-Bromofluorobenzene 104 71.4 125 51.8 50.0 BWH0811-MSD1 Toluene-dB 100 63.2 129 50.0 50.0 Surrogate Recoveries (Field Samples) LabNumber Analyte Result Spklvl ¾Rec LCL UCL 8260 Low Level Volatiles 22H1255-03 Toluene-dB 22H1255-03 4-Bromofluorobenzene 22H1255-03 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22H1255-07 Toluene-dB 22H1255-07 22H1255-07 4-Bromofluorobenzene 1,2-Dichloroethane-d4 CtF WO#: 22H1255 www.ChemtechFord.com 10.3 10.2 10.3 10.2 10.3 10.2 10.0 10.0 10.0 10.0 10.0 10.0 103 102 103 102 103 102 63.2 129 71.4 125 64.2 126 63.2 129 71.4 125 64.2 126 Batch OF BWH0811 1.00 BWH0811 1.00 BWH0811 1.00 BWH0811 1.00 BWH0811 1.00 BWH0B11 1.00 BWH0B11 1.00 BWH0811 1.00 BWH0811 1.00 BWH0811 1.00 BWH0B11 1.00 BWH0811 1.00 Qualifier Page 20 of 20 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD LA801to\TOjtlti Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-11_09212022 Matrix: Water Date Sampled: 9/21/22 10:30 l11111·1!ani,· Chloride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \ktal, Manganese, Dissolved Result 68.1 2.65 1300 2280 0.212 Project Name: September Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 1.0 0.100 20.0 20 0,0100 PO#: Receipt: 9/23/22 11 :20@ -0.3 ·c Date Reported: 10/6/2022 Project Name: September Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 EPA300.0 SM 2540C EPA200.8 CtF WO#: 2212016 Preparation Date/Time 9/30/22 9/23/22 10/4/22 9/28/22 9/29/22 Lab ID: 2212016-01 Analysis Date/Time 10/1/22 9/23/22 10/4/22 9/28/22 9/29/22 Flag(s) Page 3 of 19 Chemtech-Ford Laboratories CHEMTECH-FORD li\ft.OiAfOIIIU.S Energy Fuels Resources, Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 MW-25_09202022 Water 9/20/22 13:45 2750 September Ground Water 2022 Certificate of Analysis 20 9/23/22 11 :20@ -0.3 °C September Ground Water 2022 Tanner Holliday SM2540 C 2212016 Page 4 of 19 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA8O1U,T0RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-26_09202022 Matrix: Water Date Sampled: 9/20/22 10:45 lnurj!anit Chloride Nitrate+ Nitrite, Total, as N \olatilt· (lr!,!allll ( omp1111111h Chloroform Result 62.1 0.491 810 Project Name: September Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L ug/L Certificate of Analysis Minimum Reporting Limit 1.0 0.100 100 PO#: Receipt: 9/23/22 11 :20@ -0.3 ·c Date Reported: 10/6/2022 Project Name: September Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 EPA 8260D /5030A CtF WO#: 2212016 Preparation Date/Time 9/30/22 9/23/22 9/30/22 Lab ID: 2212016-03 Analysis Date/Time 10/1/22 9/23/22 9/30/22 Page 5 of 19 Chemtech-Ford Laboratories www.ChemtechFord.com CHEMTECH·FORD LAB:ORATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 UT 84511 MW-30_09202022 Water 9/20/22 10:00 lnoq,!anil' September Ground Water 2022 www.ChemtechFord.com mg/L mg/L mg/L mg/L Certificate of Analysis 9/23/22 11 :20@ -0.3 September Ground Water 2022 Tanner Holliday 2212016 Page 6 of 19 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LASORAT0RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-31_09202022 Matrix: Water Date Sampled: 9/20/22 12:50 lnnrJ!alli!' Chloride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) Uranium, Dissolved 390 17. l 1200 2830 0.0188 Project Name: September Ground Water 2022 www. Chem tech Ford. com Units mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting 1l.m.i! 5.0 0.500 100 20 0.0003 PO#: Receipt: 9/23/22 11 :20 @ -0.3 ·c Date Reported: 10/6/2022 Project Name: September Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 CtF WO#: 2212016 Preparation Date/Time I 0/4/22 9/23/22 I 0/4/22 9/27/22 9/29/22 Lab ID: 2212016-05 Analysis Date/Time 10/5/22 9/23/22 10/4/22 9/27/22 9/29/22 Page 7 of 19 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD LA8OFl:,H0 RI E5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-65_09202022 Matrix: Water Date Sampled: 9/20/22 13:45 Project Name: September Ground Water 2022 www.ChemtechFord.com Certificate of Analysis PO#: Receipt: 9/23/22 11 :20@ -0.3 °C Date Reported: 10/6/2022 Project Name: September Ground Water 2022 Sampled By: Tanner Holliday CtF WO#: 2212016 Lab ID: Page 8 of 19 Chemtech-Ford Laboratories CHEMTECH·FORD LA6ORAT0IIIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Trip Blank Water 9/22/22 11:20 September Ground Water 2022 Certificate of Analysis 9/23/22 11 :20@ -0.3 °C September Ground Water 2022 Tanner Holliday 2212016 Page 9 of 19 Client Service Contact: 801.262. 7299 Serving the lntermountain West since 1953 www.ChemtechFord.com Page 1 of 19 Energy Fuels Resources, Inc. Project: September Ground Water 2022 Project Manager: Tanner Holliday Laboratory ID 2212016-01 2212016-02 2212016-03 2212016-04 2212016-05 2212016-06 2212016-07 Sample Name MW-11_09212022 MW-25_09202022 MW-26 _ 09202022 MW-30 _ 09202022 MW-31 _09202022 MW-65_09202022 Trip Blank Work Order Report Narrative Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions There are no corrective actions associated with this work order. Project Name: September Ground Water 2022 www.ChemtechFord.com CtF WO#: 2212016 Page 2 of 19 CHEMTECH-FORD LA80FO,TORIES Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Certificate of Analysis Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations ND = Not detected at the corresponding Minimum Reporting Limit (MRL). PO#: Receipt: 9/23/22 11 :20@ -0.3 ·c Date Reported: 10/6/2022 Project Name: September Ground Water 2022 I mg/L = one milligram per liter or I mg/kg = one milligram per kilogram = I part per million I ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = I part per billion. I ng/L = one nano gram per liter or I ng/kg = one nano gram per kilogram = I part per trillion_ Project Name: September Ground Water 2022 www.ChemtechFord.com CtF WO#: 2212016 Page 10 of 19 3 5 6 8 2 � Client: Address: Contact: Phone#: Email: Project Name: Project#: PO#: Sampler Name: IIW-11_09212022 IIW-25_09202022 IIW-26 09202022 IIW-30_09202022 IIW-31_09202022 IIW-65_09202022 Trip Blank ;).;) ����n West Analytical Laboratories 463 W. 3600 s. Salt Lake City. UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 Fax# (801) 263-8687 Email awal@awal�abs.com www.awal-labs.com Energy Fuel.a Resources, Inc. 6425 8. Hwy. 191 Blanding, UT 84511 Tanner Holliday (435)678-2221 Cell#: tholllda�eq:,faela.com; nel.Del'ii'-afuela.com; September Ground Water 2022 Tanner Holliday Date SamolelD: Samoled 9/21/2022 9/20/2022 9/20/2022 9/20/2022 9/20/2022 9/20/2022 9/20/2022 R<lllnquisl>ed by: } .,,__._ l,11111/rr ,Jf-:./ JI..//)/ �"'4/ftltnl. '"""' Print Name: Tanner Hollfdav 11"" -nqulohod by: Dale: "'"-••- [Time: Print Name: Relinquished by: Date: �--··-I""''" 0rintName· Rellnqulahed by: IO•te: � ........... rrme: ,IN.,,,.-: CHAIN OF CUSTODY All analysis wm be conducted uelng NELAP acc,edlted methods and all data will be n,ported using AWAL'o standard analyte roots and r1lpOf1ing limits (POL) unless apecifi<ally ,_led olhefwiae on thia Chain of CuslDdy and/or attached doo.Jrnerrtalion. AWl'J.. Lab Sample Set# Page of I QC Level: I3 iiic:i iiic:i "' --0 r:--"' 0 --0 r-: £!. 0 0 •£!. •• j � 5 C, It c:i 1:i 5 0 "l � !:l. lll ... � ,. 0 C ·c: I') "II "II � ! i • 0 "' ! .t 0 It) It) � -i �iTime Q. N !0 E 0 u Samoled ., i5 i5 .. "' I: .. 1030 4 w X X X 1346 I w X 1045 5 w X X 1000 3 w X X X 1250 4 w X X X X 1346 I w X 1045 3 w - RecelV� an,, -:;,.: �_;> L,.," e,. IPnnt .. ame· R.-edby: ls-.. PttnlName: R-.ed by: ls ..... tun, IPrtnt Neme: Received by: le:....••- Tum Around Time: Standard �� � c:i c:i c::i 0 0 0 ('I rs rs ;::: ;::: ;::: c::i ci' c:i c:i 0 0 0 0 � IO� � rs • 9 •� J II C, i 5 c:i ! a 111 0 "II .! 5 "l � ,. ii ... 0 u lll 0 0 0 "II "II "II 0 :a II II !It) .t .t u� i i i • i g i5 iS iS X X X X X X 0tf'�3 iJI) nme ,\ \ Q_ 't) Date: rtme: Dale: fnme: Oata; Uni.... 0-amongements hlYO _, made, signed repo'1B wll be emaled by 5:00 pm on Iha day lhey are due. X Include EDD: LOCUB UPLOAD BXCEJ. X Field Filtered For: DtaaolYNlletala For Compliance With: □NELAP □RCRA□CWA □SOWA □ELAP/A2LA □NLLAP □Non-Compliance □Other: Known Hazards & Samole Comments QC.. QC.. Special Instructions: Due D�lc: Laboratory Use Only �ampleeW-: 1 Shipped °' hand delivered 2 Aml,;ent °' Chilled 3 T---Q.:3._ -c 4 -ed Btcunlleeldng ('"""-1)- Sealed) y N 5 Property p,_.,ed y N C-ed at bench y N 6 Roceived Within Holding TI.,_ y N 1 bonOuterP-- Y N NA oonOuterP-- Y N NA 3 p,_..ton Sample y N NA 4 Unbrok-, on Sample y N NA -SampleILabeia and COC Reoord? N Sample containers for metals were field filtered. See the Analytical Scope of Work for Reporting Limits and VOC analyte list. fllme: Page 11 of 1 ....._.N..,.· . 9 l 2.. \ )7 Work Order # dct :S::: �D � (.('.) Delivery Method: 61..JPS D USPS d Ch h C D Fe Ex D emtec ouner D Walk-in D Customer Courier '{ '-4 '../ 0 � q 7 I t.{ 9 <, 5'{ -Olemtech Lot I Sample# Container Preservative 6'1. �� \\ 0 \\%� N' \S,. \ l n (V'\ \\ �L, �� A\.-.. "� �("") \\� -� ,, l::.l \ ln ,�L�) \ J. o, I'\ tJ n.�tl%-� tJ lol\C.O 1'--1'. \\ �V) ,...,� �V\ ,�o \ \i8' ...__ \ ' I� I {,. 'Iv\... l\ ?u ()(. A-� �, we...�'\ I !:' � .. .8 ... l! i u � a. ;: C iiix .. ..D i5 u cc � j; .E 'a ... il i � i!:.. E ;: � I .;. .i j;J! .. Misc G: l Volume �(o,/ml) � CHEMTECH FORD LABORATORIES Sample Receipt Receiving Temperature -o.3 °C - Comments �o \o� No l&� No \--� \.\W tt. - ,.,, _,. \ '2( \_l 0 v:,...9; \o f-.)e lo.\- �o \o� CHEMTECH-FORD L-\8(\!IATORl[S Sample Condition ( check if yes ) C can be matched to bottles SuHicent Sample Volume Plastic Containers A· Plastic Unpreserved 8- Misceltaneous Plastic C· Cvanide Qt (NaOH) E• Coliform/Ecoli/HPC F- Sutfide Qr (Zn Acetate} L-Mercury 1631 M· Metals Pint (HN03) N• Nutrient Pint (H2S04) R- Radiological (HN03) S- Sludge Cups/rubs Q- Plastic Bag Glass Containers 0- 625 (Na2S203) G· Glass Unpreserved H· HAAs (NH4CI) I· 508/515/525 (Na2503) K· 51S.3 Herbicides O· Oil & Grease (HCI) p. Phenols (H2S04) T-TOC/rOX (H3P04) U· 531 (MCAA, Na2S203) V• 524/rHMs (Ascorbic Acid) W- 8260 voe (1:1 HCI) X· Vial Unpreserved Y- 624/504 (Na25203) z. Miscellaneous Glass Page 12 of 19 2212016 QC Report for Work Order (WO) -2212016 Blank -EPA 200.8 0.0100 1.00 0.0050 1.00 0.0003 1.00 LCS -EPA 200.8 100 85 -115 0.040 0.0400 0.0005 1.00 102 85 -115 0.041 0.0400 0.0005 1.00 101 85 -115 0.041 0.0400 0.0003 1.00 Matrix Spike -EPA 200.8 104 70 -130 0.055 0.013 0.0400 0.0005 1.00 106 70 -130 0.043 0.0002 0.0400 0.0005 1.00 73.2 70 -130 0.029 0.0400 0.0003 1.00 98.9 70 -130 0.040 0.0400 0.0005 1.00 105 70 -130 0.045 0.003 0.0400 0.0005 1.00 109 70 -130 0.044 0.0001 0.0400 0.0003 1.00 95.0 70 -130 0.250 0.212 0.0400 0.0005 1.00 108 70 -130 0.059 0.016 0.0400 0.0005 1.00 92.5 70-130 0.039 0.002 0.0400 0.0003 1.00 Page 13 of 19 QC Report for Work Order (WO) -2212016 Analyte % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -EPA 300.0 QC Sample ID: BWI1594-BLK1 Batch: BWI1594 Date Prepared: 09/30/2022 Date Analyzed: 10/01/2022 Units: mg/L Chloride ND 1.0 1.00 QC Sample ID: BWJ0073-BLK1 Batch: BWJ0073 Date Prepared: 10/04/2022 Date Analyzed: 10/04/2022 Units: mg/L Sulfate ND 1.0 1.00 QC Sample ID: BWJ0135-BLK1 Batch: BWJ0135 Date Prepared: 10/04/2022 Date Analyzed: 10/05/2022 Units: mg/L Chloride ND 1.0 1.00 LCS -EPA 300.0 QC Sample ID: BWil594-BSl Batch: BWil 594 Date Prepared: 09/30/2022 Date Analyzed: I 0/0 I /2022 Units: mg/L Chloride 96.1 90 -110 48.1 50.0 1.0 1.00 QC Sample ID: BWJ0073-BSl Batch: BWJ0073 Date Prepared: 10/04/2022 Date Analyzed: 10/04/2022 Units: mg/L Sulfate 99.1 90 - 110 49.5 50.0 1.0 1.00 QC Sample ID: BWJ0135-BSI Batch: BWJOl35 Date Prepared: 10/04/2022 Date Analyzed: I 0/05/2022 Units: mg/L Chloride 97.6 90 -110 48.8 50.0 1.0 1.00 Matrix Spike -EPA 300.0 QC Sample ID: BWl1594-MS1 Batch: BWI1594 QC Source Sample: 2212016-01 Date Prepared: 09/30/2022 Date Analyzed: 10/0 l /2022 Units: mg/L Chloride 74.7 80 -120 76.4 68.1 11.1 1.1 1.00 QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWI1594-MS2 Batch: BWI1594 QC Source Sample: 22(2016-03 Date Prepared: 09/30/2022 Date Analyzed: I 0/0 I /2022 Units: mg/L Chloride 92.7 80 -120 72.4 62.1 11.1 1.1 1.00 QC Sample ID: BWJ0073-MS1 Batch: BWJ0073 QC Source Sample: 2212016-0 I Date Prepared: 10/04/2022 Date Analyzed: 10/04/2022 Units: mg/L Sulfate 68.6 80 -120 1440 1300 200 22.0 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWJ0073-MS2 Batch: BWJ0073 QC Source Sample: XXXXXXX-XX Date Prepared: I 0/04/2022 Date Analyzed: l 0/04/2022 Units: mg/L Sulfate -1850 80 -120 ND 185 10.0 1.0 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). QC Sample ID: BWJ0135-MS1 Batch: BWJ0135 QC Source Sample: XXXXXXX-XX Date Prepared: 10/04/2022 Date Analyzed: 10/05/2022 Units: mg/L Chloride 99.7 80 -120 36.3 25.2 11.1 1.1 1.00 QC Sample JD: BWJ0135-MS2 Batch: BWJ0135 QC Source Sample: XXXXXXX-XX Date Prepared: 10/04/2022 Date Analyzed: 10/05/2022 Units: mg/L Chloride 97.6 80 -120 45.4 34.5 11.1 1.1 1.00 CtF WO#: 2212016 www.ChemtechFord.com Page14of19 QC Report for Work Order (WO) -2212016 Analyte % Rec RPO Limits RPO Max Result Source Cone Matrix Spike Dup - EPA 300.0 QC Sample ID: BWil594-MSD1 Batch: BWI1594 QC Source Sample: 2212016-0 I Date Prepared: 09/30/2022 Date Analyzed: I 0/01/2022 Units: mg/L Chloride 89.2 2.09 80 -120 20 78.0 68.1 QC Sample ID: BWil594-MSD2 Batch: BWil594 QC Source Sample: 2212016-03 Date Prepared: 09/30/2022 Date Analyzed: 10/01/2022 Units: mg/L Chloride 93.3 0.105 80 -120 20 72.4 62.1 QC Sample ID: BWJ0073-MSD1 Batch: BWJ0073 QC Source Sample: 2212016-01 Date Prepared: 10/04/2022 Date Analyzed: 10/04/2022 Units: mg/L Sulfate 60.6 1.12 80 -120 20 1420 1300 QM-4X - The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWJ0073-MSD2 Batch: BWJ0073 QC Source Sample: XXXXXXX-XX Date Prepared: 10/04/2022 Date Analyzed: I 0/04/2022 Units: Sulfate -1850 80 -120 20 ND 185 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag}. QC Sample ID: BWJ0135-MSDI Date Prepared: I 0/04/2022 Chloride QC Sample ID: BWJ0135-MSD2 Date Prepared: 10/04/2022 Chloride CtF WO#: 2212016 www.ChemtechFord.com Batch: BWJ0135 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/05/2022 Units: 101 0.378 80 -120 20 36.4 25.2 Batch: BWJ0135 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/05/2022 Units: 99.1 0.367 80 - 120 20 45.6 34.5 mg/L mg/L mg/L Spk Value MRL DF 11.1 1.1 1.00 11.1 1.1 1.00 200 22.0 1.00 10.0 1.0 1.00 11.1 1.1 1.00 11.1 1.1 1.00 Page 15 of 19 Analyte QC Sample ID: BWI1260-BLKI Date Prepared: 09/23/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWI1260-BS1 Date Prepared: 09/23/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWI1260-MSI Date Prepared: 09/23/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWJ1260-MS2 Date Prepared: 09/23/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWl1260-MSDI Date Prepared: 09/23/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWI1260-MSD2 Date Prepared: 09/23/2022 Nitrate+ Nitrite, Total, as N CtF WO#: 2212016 www.ChemtechFord.com QC Report for Work Order (WO) -2212016 %Rec RPD Limits RPD Max Result Source Cone Blank -EPA 353.2 Batch: BWI1260 Date Analyzed: 09/23/2022 Units: mg/L ND LCS -EPA 353.2 Batch: BWI1260 Date Analyzed: 09/23/2022 Units: mg/L 98.5 80 -120 1.97 Matrix Spike -EPA 353.2 Batch: BW11260 QC Source Sample: 2212016-01 Date Analyzed: 09/23/2022 Units: mg/L 99.4 80 - 120 3.65 2.65 Batch: BWl1260 QC Source Sample: 2212016-03 Date Analyzed: 09/23/2022 Units: mg/L 91.8 80 - 120 1.41 0.491 Matrix Spike Dup - EPA 353.2 Batch: BW11260 QC Source Sample: 2212016-01 Date Analyzed: 09/23/2022 Units: mg/L 84.5 4.17 80-120 20 3.50 2.65 Batch: BWil260 QC Source Sample: 22120 I 6-03 Date Analyzed: 09/23/2022 Units: mg/L 90.4 0.999 80 -120 20 1.40 0.491 Spk Value MRL DF 0.100 1.00 2.00 0.100 1.00 1.00 0.100 1.00 1.00 0.100 1.00 1.00 0.100 1.00 1.00 0.100 1.00 Page16of19 QC Report for Work Order (WO) -2212016 Analyte %Rec RPO Limits RPO Max Result Source Cone Blank -EPA 8260D /5030A QC Sample ID: BWJ0002-BLKI Batch: BWJ0002 Date Prepared: 09/30/2022 Date Analyzed: 09/30/2022 Units: Acetone ND Benzene ND Carbon Tetrachloride ND Chloroform ND Chloromethane ND J-LOW -Estimated low due to low recovery of LCS or CCV Methyl Ethyl Ketone ND Methylene Chloride ND J-LOW -Estimated low due to low recovery of LCS or CCV Naphthalene ND Tetrahydrofuran ND Toluene ND Xylenes, total ND LCS -EPA 8260D /5030A QC Sample ID: BWJ0002-BS1 Batch: BWJ0002 Date Prepared: 09/30/2022 Date Analyzed: 09/30/2022 Units: Chloroform 83.8 70-130 8.38 Matrix Spike -EPA 8260D /5030A QC Sample ID: BWJ0002-MSI Batch: BWJ0002 QC Source Sample: 2212016-03 Date Prepared: 09/30/2022 Date Analyzed: 09/30/2022 Units: Chloroform -6790 70 -130 131 810 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Matrix Spike Dup -EPA 8260D /5030A QC Sample ID: BWJ0002-MSD1 Batch: BWJ0002 QC Source Sample: 2212016-03 Date Prepared: 09/30/2022 Date Analyzed: 09/30/2022 Units: Chloroform -6810 -0.279 70 -130 20 129 810 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. CtF WO#: 2212016 www.ChemtechFord.com ug/L ug/L ug/L ug/L Spk Value MRL OF 20.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 20.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 Page 17 of 19 2212016 www.ChemtechFord.com QC Report for Work Order (WO) -2212016 Blank -SM 2540 C Duplicate -SM 2540 C 10 10 LCS -SM 2540 C 90-110 Page 18 of 19 Surrogates Report for Work Order (WO) -2212016 QCID Analyte % Rec LCL UCL Result Spk Value Blank -EPA 82600 /5030A BWJ0002-BLK1 1,2-Dichloroethane-d4 110 64.2 126 11.0 10.0 BWJ0002-BLK1 4-Bromofluorobenzene 99.7 71.4 125 9.97 10.0 BWJ0002-BLK1 Toluene-dB 100 63.2 129 10.0 10.0 LCS -EPA 82600 /5030A BWJ0002-BS1 1,2-Dichloroethane-d4 108 64.2 126 10.8 10.0 BWJ0002-8S1 4-Bromofluorobenzene 99.5 71.4 125 9.95 10.0 BWJ0002-8S1 Toluene-dB 99.5 63.2 129 9.95 10.0 Matrix Spike -EPA 82600 /5030A BWJ0002-MS1 1,2-Dichloroethane-d4 107 64.2 126 10.7 10.0 BWJ0002-MS1 4-Bromofluorobenzene 98.6 71.4 125 9.86 10.0 BWJ0002-MS1 Toluene-dB 100 63.2 129 10.0 10.0 Matrix Spike Cup -EPA 82600 /5030A BWJ0002-MSD1 1,2-Dichloroethane-d4 108 64.2 126 10.8 10.0 BWJ0002-MSD1 4-Bromofluorobenzene 98.8 71.4 125 9.88 10.0 BWJ0002-MSD1 Toluene-dB 100 63.2 129 10.0 10.0 Surrogate Recoveries (Field Samples) LabNumber Analyte Result Spklvl %Rec LCL UCL 8260 Low Level Volatiles 2212016-03 Toluene-dB 2212016-03 4-Bromofluorobenzene 2212016-03 1,2-Dichloroethane-d4 8260 Low Level Volatiles 2212016-07 Toluene-dB 2212016-07 2212016-07 4-Bromofluorobenzene 1,2-Dichloroethane-d4 CtF WO#: 2212016 www.ChemtechFord.com 10.0 10.1 10.5 10.0 10.0 9.76 10.0 10.0 10.0 10.0 10.0 10.0 100 101 105 100 100 97.6 63.2 129 71.4 125 64.2 126 63.2 129 71.4 125 64.2 126 Batch OF BWJ0002 1.00 BWJ0002 1.00 BWJ0002 1.00 BWJ0002 1.00 BWJ0002 1.00 BWJ0002 1.00 BWJ0002 1.00 BWJ0002 1.00 BWJ0002 1.00 BWJ0002 1.00 BWJ0002 1.00 BWJ0002 1.00 Qualifier Page 19 of 19 G 1 A Q rt I F Id QA/QC E I -ua er✓ 1e va uation 1x Casing 2x Casing Location Volume Volume Pumped Volume Volume Check Conductivity RPO pH RPO Temperature RPD Redox RPO Turbidity RPO Dissolved Oxygen RPO MW-11 29.18 58.59 58.36 okay 3190 3184 0.19 7.53 7.52 0.13 15.12 15.10 0.13 350 347 0.86 107.0 110.0 2.76 4.0 4.2 4.88 MW-12 13.60 28.21 27.2 okay 4165 4163 0.05 6.87 6.87 0.00 15.72 15.73 0.06 252 253 0.40 0 0 0.00 31.0 31.4 1.28 MW-14 17.61 39.06 35.22 okay 3898 3894 0.10 6.72 6.72 0.00 14.38 15.30 6.20 324 324 0.00 1.4 1.5 6.90 1.1 1.1 0.00 MW�24 6185 I 14.00 13..7 Pumped Dry,· _447,5 4477 0,04 4.88 4,89 0.20 16.S0 16.38 Q.73 _ I•NM � NC NM NO -NM NC MW-2.4 6.94 � 14-.40 13.88 PumJ:)8(1 Dry-4476 4483 (!).16 4.78 4.80 0.42 16.20 16.15 0.31 NM NO NM � ,·NC NM NO MW•24A 7.45 15.38 14.9 PUml).8!;1 Dry 4431 4446 0.34 4.88 4-�0.41 15.75 15.70 0.32 NM NG NM NC NM NC MW-25 21.53 45.57 43.06 okay 3185 3190 0.16 6.99 6.98 0.14 15.25 15.16 0.59 361 361 0.00 2.1 2.0 4.88 4.5 4.6 2.20 MW-26 NA Continuously Pumped well -34"69 NC 7.20 NC 16.50 NC 317 NC 0 NC 41.4 NC MW-27 23.73 49.91 47.46 okay 1220 1202 1.49 7.69 7.69 0.00 15.70 15.67 0.19 314 314 0.00 0 0 0.00 97.0 97.3 0.31 MW-28 23.08 46.65 46.16 okay 4239 4230 0.21 6.71 6.70 0.15 15.85 15.79 0.38 296 295 0.34 2.0 2.0 0.00 34.9 34.5 1.15 MW-29 ' 18.27 39.06 36.54 okay 4501 4540 0.86 6.65 6.64 0.15 15.75 15.65 0.64 222 221 0.45 14.0 13.0 7.41 1.2 1.1 8.70 MW-30 22.60 45.57 45.2 okay 2238 2237 0.04 7.33 7_33· 0.00 15.06 15.00 0.46 365 364 0.27 0 0 0.00 52.0 52.5 0.96 MW-31 39.40 79.20 78.8 okay 3418 3440 0.64 7.30 7.28 0.27 15.45 15.43 0.13 338 337 0.30 0 0 0.00 115.0 115.0 0.00 MW-32 31.14 65.10 62.28 okay 3724 3722 0.05 6.67 6 .. 65 0.30 15.44 15.43 0.06 216 216 0.00 5.2 5.2 0.00 6.9 6.8 1.46 MW-36 7.21 15.19 14.42 okay 4763 4841 1.62 7.12 7.11 0.14 15.70 15.74 0.25 351 350 0.29 1.0 1.0 0.00 81.0 83.0 2.44 MW-38 2.73 � 5.00 5.46 Pumped Ory 4300 4297 0.01 6.70 6.71 (:).15 16.50 16.40 0.81 NM NC NM NC NM NC MW-39 24.78 49.91 49.56 okay 4810 4811 0.02 4.30 4.28 0.47 15.35 15.34 0.07 422 434 2.80 0 0 0.00 4.0 4.0 0.00 MW-40 26.21 53.16 52.42 okay 3880 3890 0.26 7.18 7.17 0.14 15.25 15.23 0.13 256 259 1.17 0 0 0.00 106.3 106.7 0.38 MW-26 rs a continually pumped well. W-24 MW•24A M -38 were ,um ed dry a d sam led after rec®e____ _.._ ____________________________________________ ...... _______________________ NM = Not Measured. The QAP does not require the measurement of redox potential or turbidity in wells that were purged to dryness. RPD = Relative Percent Difference The OAP states that turbidity should be less than 5 Nephelometric Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU are included for information purposes only. G-18: Accelerated Field QA/QC Evaluation 1x Casing 2x Casing Volume Location Volume Volume Pumped Volume Check Conductivity RPD pH MW-11 29.15 58.59 58.3 okay 3060 I 3059 0.03 7.61 I MW-25 21.53 45.57 43.06 okay 3145 I 3149 0.13 7.07 I MW-26 NA Continuously Pumped well --3462 NC 7.02 MW-30 22.59 45.57 45.18 okay 2234 I 2230 0.18 7.34 I MW-31 39.37 80.29 78.74 okay 3436 I 3437 0.03 7.36 I MW-11 29.20 58.59 58.4 okay 3051 I 3067 0.52 7.05 I MW-25 21.53 45.57 43.06 okay 3170 I 3171 0.03 6.61 I MW-26 NA Continuously Pumped well --3536 NC 6.69 MW-30 22.65 45.57 45.3 okay 2250 I 2249 0.04 6.80 I MW-31 39.44 80.29 78.88 okay 3422 I 3428 0.18 6.66 I MW-26, Is a continually pumped well. here are no wells that were · um d d , NM= Not Measured. The QAP does not require the measurement of redox potential or turbidity in wells that were purged to dryness. RPO= Relative Percent Difference August RPD 7.61 0.00 7.06 0.14 NC 7.33 0.14 7.35 0.14 September 7.08 0.42 6.62 0.15 NC 6.81 0.15 6.70 0.60 Dissolved Temperature RPD Redox RPD Turbidity RPO Ox11gen 15,iO I 15.19 0.59 308 I 307 0.33 126.0 I 121.0 0.79 4.0 3.9 15.72 I 15.70 0.13 313 I 313 0.00 1.0 I 1.0 0.00 3.4 3.4 18.20 NC 254 NC 2.0 NC 35.0 15.49 I 15.48 0.06 306 I 306 0.00 0 I 0 0.00 54.0 54.0 15.43 I 15.44 0.06 293 I 293 0.00 1.9 I 1.8 5.41 114.3 114.5 14.70 I 14.73 0.20 417 I 416 0.24 2.0 I 2.1 4.88 1.0 1.0 15.12 I 15.07 0.33 334 I 334 0.00 0 I 0 0.00 4.1 4.1 16.11 NC 373 NC 0 NC 28.4 14.82 I 14.80 0.14 414 I 413 0.24 0 I 0 0.00 53.9 54.0 15.23 I 15.21 0.13 331 I 330 0.30 0 I 0 0.00 111.9 111.5 The OAP states that turbidity should be less than 5 Nephelometric Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU are included for information purposes only. RPD 2.53 0.00 NC 0.00 0.17 0.00 0.00 NC 0.19 0.36 G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check Trip Blank Acetone 7/12/2022 7/18/2022 6 14 OK Trip Blank Benzene 7/12/2022 7/18/2022 6 14 OK Trip Blank Carbon Tetrachloride 7/12/2022 7/18/2022 6 14 OK Trip Blank Chloroform 7/12/2022 7/18/2022 6 14 OK Trip Blank Chloromethane 7/12/2022 7/18/2022 6 14 OK Trip Blank Methyl Ethyl Ketone 7/12/2022 7/18/2022 6 14 OK Trip Blank Methylene Chloride 7/12/2022 7/18/2022 6 14 OK Trip Blank Naphthalene 7/12/2022 7/18/2022 6 14 OK Trip Blank Tetrahydrofuran 7/12/2022 7/18/2022 6 14 OK Trip Blank Toluene 7/12/2022 7/18/2022 6 14 OK Trip Blank Xylenes, total 7/12/2022 7/18/2022 6 14 OK Trip Blank Acetone 7/19/2022 7/30/2022 11 14 OK Trip Blank Benzene 7/19/2022 7/30/2022 11 14 OK Trip Blank Carbon Tetrachloride 7/19/2022 7/30/2022 11 14 OK Trip Blank Chloroform 7/19/2022 7/30/2022 11 14 OK Trip Blank Chloromethane 7/19/2022 7/30/2022 11 14 OK Trip Blank Methyl Ethyl Ketone 7/19/2022 7/30/2022 11 14 OK Trip Blank Methylene Chloride 7/19/2022 7/30/2022 11 14 OK Trip Blank Naphthalene 7/19/2022 7/30/2022 11 14 OK Trip Blank Tetrahydrofuran 7/19/2022 7/30/2022 11 14 OK Trip Blank Toluene 7/19/2022 7/30/2022 11 14 OK Trip Blank Xylenes, total 7/19/2022 7/30/2022 11 14 OK MW-11 Acetone 7/12/2022 7/18/2022 6 14 OK MW-11 Arsenic 7/12/2022 7/29/2022 17 180 OK MW-11 Benzene 7/12/2022 7/18/2022 6 14 OK MW-11 Beryllium 7/12/2022 7/29/2022 17 180 OK MW-11 Bicarbonate as CaCO3 7/12/2022 7/19/2022 7 14 OK MW-II Cadmium 7/12/2022 7/29/2022 17 180 OK MW-11 Calcium 7/12/2022 7/28/2022 16 180 OK MW-II Carbon Tetrachloride 7/12/2022 7/18/2022 6 14 OK MW-11 Carbonate as CO3 7/12/2022 7/19/2022 7 14 OK MW-11 Chloride 7/12/2022 7/16/2022 4 28 OK MW-11 Chloroform 7/12/2022 7/18/2022 6 14 OK MW-11 Chloromethane 7/12/2022 7/18/2022 6 14 OK MW-11 Chromium 7/12/2022 7/29/2022 17 180 OK MW-11 Cobalt 7/12/2022 7/29/2022 17 180 OK MW-11 Copper 7/12/2022 7/29/2022 17 180 OK MW-11 Fluoride 7/12/2022 7/16/2022 4 28 OK MW-11 Gross Radium Alpha 7/12/2022 8/19/2022 38 180 OK MW-11 Iron 7/12/2022 7/28/2022 16 180 OK MW-11 Lead 7/12/2022 7/29/2022 17 180 OK MW-11 Magnesium 7/12/2022 7/28/2022 16 180 OK MW-11 Manganese 7/12/2022 7/29/2022 17 180 OK MW-11 Mercury 7/12/2022 7/21/2022 9 180 OK MW-11 Methyl Ethyl Ketone 7/12/2022 7/18/2022 6 14 OK MW-11 Methylene Chloride 7/12/2022 7/18/2022 6 14 OK MW-11 Molybdenum 7/12/2022 7/29/2022 17 180 OK MW-11 Naphthalene 7/12/2022 7/18/2022 6 14 OK MW-11 Nickel 7/12/2022 7/29/2022 17 180 OK MW-11 Nitrate + Nitrite as N 7/12/2022 7/27/2022 15 28 OK MW-11 Nitrogen, Ammonia as N 7/12/2022 7/26/2022 14 28 OK MW-11 Potassium 7/12/2022 7/28/2022 16 180 OK MW-11 Selenium 7/12/2022 7/29/2022 17 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-11 Silver 7/12/2022 7/29/2022 17 180 OK MW-11 Sodium 7/12/2022 7/28/2022 16 180 OK MW-11 Sulfate 7/12/2022 8/1/2022 20 28 OK MW-11 Tetrahydrofuran 7/12/2022 7/18/2022 6 14 OK MW-11 Thallium 7/12/2022 7/29/2022 17 180 OK MW-11 Tin 7/12/2022 7/28/2022 16 180 OK MW-11 Toluene 7/12/2022 7/18/2022 6 14 OK MW-11 Total Dissolved Solids 7/12/2022 7/18/2022 6 7 OK MW-II Uranium 7/12/2022 7/29/2022 17 180 OK MW-II Vanadium 7/12/2022 7/29/2022 17 180 OK MW-11 Xvlenes, total 7/12/2022 7/18/2022 6 14 OK MW-11 Zinc 7/12/2022 7/29/2022 17 180 OK MW-12 Selenium 7/14/2022 8/1/2022 18 180 OK MW-12 Uranium 7/14/2022 8/1/2022 18 180 OK MW-14 Acetone 7/13/2022 7/18/2022 5 14 OK MW-14 Arsenic 7/13/2022 7/29/2022 16 180 OK MW-14 Benzene 7/13/2022 7/18/2022 5 14 OK MW-14 Beryllium 7/13/2022 7/29/2022 16 180 OK MW-14 Bicarbonate as CaCO3 7/13/2022 7/19/2022 6 14 OK MW-14 Cadmium 7/13/2022 7/29/2022 16 180 OK MW-14 Calcium 7/13/2022 7/28/2022 15 180 OK MW-14 Carbon Tetrachloride 7/13/2022 7/18/2022 5 14 OK MW-14 Carbonate as CO3 7/13/2022 7/19/2022 6 14 OK MW-14 Chloride 7/13/2022 7/16/2022 3 28 OK MW-14 Chloroform 7/13/2022 7/18/2022 5 14 OK MW-14 Chloromethane 7/13/2022 7/18/2022 5 14 OK MW-14 Chromium 7/13/2022 7/29/2022 16 180 OK MW-14 Cobalt 7/13/2022 7/29/2022 16 180 OK MW-14 Coooer 7/13/2022 7/29/2022 16 180 OK MW-14 Fluoride 7/13/2022 7/16/2022 3 28 OK MW-14 Gross Radium Alpha 7/13/2022 8/17/2022 35 180 OK MW-14 Iron 7/13/2022 7/28/2022 15 180 OK MW-14 Lead 7/13/2022 7/29/2022 16 180 OK MW-14 Magnesium 7/13/2022 7/28/2022 15 180 OK MW-14 Manganese 7/13/2022 7/29/2022 16 180 OK MW-14 Mercury 7/13/2022 7/21/2022 8 180 OK MW-14 Methyl Ethyl Ketone 7/13/2022 7/18/2022 5 14 OK MW-14 Methylene Chloride 7/13/2022 7/18/2022 5 14 OK MW-14 Molybdenum 7/13/2022 7/29/2022 16 180 OK MW-14 Naphthalene 7/13/2022 7/18/2022 5 14 OK MW-14 Nickel 7/13/2022 7/29/2022 16 180 OK MW-14 Nitrate+ Nitrite as N 7/13/2022 7/26/2022 13 28 OK MW-14 Nitrogen, Ammonia as N 7/13/2022 7/26/2022 13 28 OK MW-14 Potassium 7/13/2022 7/28/2022 15 180 OK MW-14 Selenium 7/13/2022 7/29/2022 16 180 OK MW-14 Silver 7/13/2022 7/29/2022 16 180 OK MW-14 Sodium 7/13/2022 7/28/2022 15 180 OK MW-14 Sulfate 7/13/2022 8/1/2022 19 28 OK MW-14 Tetrahydrofuran 7/13/2022 7/18/2022 5 14 OK MW-14 Thallium 7/13/2022 7/29/2022 16 180 OK MW-14 Tin 7/13/2022 7/28/2022 15 180 OK MW-14 Toluene 7/13/2022 7/18/2022 5 14 OK MW-14 Total Dissolved Solids 7/13/2022 7/18/2022 5 7 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-14 Uranium 7/13/2022 7/29/2022 16 180 OK MW-14 Vanadium 7/13/2022 7/29/2022 16 180 OK MW-14 Xylenes, total 7/13/2022 7/18/2022 5 14 OK MW-14 Zinc 7/13/2022 7/29/2022 16 180 OK MW-24 Acetone 7/20/2022 7/29/2022 9 14 OK MW-24 Arsenic 7/20/2022 8/1/2022 12 180 OK MW-24 Benzene 7/20/2022 7/29/2022 9 14 OK MW-24 Beryllium 7/20/2022 8/1/2022 12 180 OK MW-24 Bicarbonate as CaCO3 7/20/2022 7/22/2022 2 14 OK MW-24 Cadmium 7/20/2022 8/1/2022 12 180 OK MW-24 Calcium 7/20/2022 8/11/2022 22 180 OK MW-24 Carbon Tetrachloride 7/20/2022 7/29/2022 9 14 OK MW-24 Carbonate as CO3 7/20/2022 7/22/2022 2 14 OK MW-24 Chloride 7/20/2022 7/22/2022 2 28 OK MW-24 Chloroform 7/20/2022 7/29/2022 9 14 OK MW-24 Chloromethane 7/20/2022 7/29/2022 9 14 OK MW-24 Chromium 7/20/2022 8/1/2022 12 180 OK MW-24 Cobalt 7/20/2022 8/1/2022 12 180 OK MW-24 Copper 7/20/2022 8/1/2022 12 180 OK MW-24 Fluoride 7/20/2022 7/22/2022 2 28 OK MW-24 Iron 7/20/2022 8/3/2022 14 180 OK MW-24 Lead 7/20/2022 8/1/2022 12 180 OK MW-24 Magnesium 7/20/2022 8/3/2022 14 180 OK MW-24 Manganese 7/20/2022 8/1/2022 12 180 OK MW-24 Mercury 7/20/2022 7/27/2022 7 180 OK MW-24 Methyl Ethyl Ketone 7/20/2022 7/29/2022 9 14 OK MW-24 Methylene Chloride 7/20/2022 7/29/2022 9 14 OK MW-24 Molybdenum 7/20/2022 8/1/2022 12 180 OK MW-24 Naphthalene 7/20/2022 7/29/2022 9 14 OK MW-24 Nickel 7/20/2022 8/1/2022 12 180 OK MW-24 Nitrate+ Nitrite as N 7/20/2022 7/29/2022 9 28 OK MW-24 Nitrogen, Ammonia as N 7/20/2022 7/26/2022 6 28 OK MW-24 Potassium 7/20/2022 8/3/2022 14 180 OK MW-24 Selenium 7/20/2022 8/1/2022 12 180 OK MW-24 Silver 7/20/2022 8/1/2022 12 180 OK MW-24 Sodium 7/20/2022 8/11/2022 22 180 OK MW-24 Sulfate 7/20/2022 7/22/2022 2 28 OK MW-24 Tetrahvdrofuran 7/20/2022 7/29/2022 9 14 OK MW-24 Thallium 7/20/2022 8/1/2022 12 180 OK MW-24 Tin 7/20/2022 8/3/2022 14 180 OK MW-24 Toluene 7/20/2022 7/29/2022 9 14 OK MW-24 Total Dissolved Solids 7/20/2022 7/22/2022 2 7 OK MW-24 Uranium 7/20/2022 8/1/2022 12 180 OK MW-24 Vanadium 7/20/2022 8/1/2022 12 180 OK MW-24 Xylenes, total 7/20/2022 7/29/2022 9 14 OK MW-24 Zinc 7/20/2022 8/1/2022 12 180 OK MW-24 Gross Radium Alpha 7/28/2022 8/19/2022 22 180 OK MW-24A Acetone 7/19/2022 7/29/2022 IO 14 OK MW-24A Arsenic 7/19/2022 8/1/2022 13 180 OK MW-24A Benzene 7/19/2022 7/29/2022 10 14 OK MW-24A Beryllium 7/19/2022 8/1/2022 13 180 OK MW-24A Bicarbonate as CaCO3 7/19/2022 7/22/2022 3 14 OK MW-24A Cadmium 7/19/2022 8/1/2022 13 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-24A Calcium 7/19/2022 8/11/2022 23 180 OK MW-24A Carbon Tetrachloride 7/19/2022 7/29/2022 10 14 OK MW-24A Carbonate as CO3 7/19/2022 7/22/2022 3 14 OK MW-24A Chloride 7/19/2022 7/22/2022 3 28 OK MW-24A Chloroform 7/19/2022 7/29/2022 10 14 OK MW-24A Chloromethane 7/19/2022 7/29/2022 10 14 OK MW-24A Chromium 7/19/2022 8/1/2022 13 180 OK MW-24A Cobalt 7/19/2022 8/1/2022 13 180 OK MW-24A Copper 7/19/2022 8/1/2022 13 180 OK MW-24A Fluoride 7/19/2022 7/22/2022 3 28 OK MW-24A Gross Radium Alpha 7/19/2022 8/17/2022 29 180 OK MW-24A Iron 7/19/2022 8/3/2022 15 180 OK MW-24A Lead 7/19/2022 8/1/2022 13 180 OK MW-24A Magnesium 7/19/2022 8/3/2022 15 180 OK MW-24A Manganese 7/19/2022 8/1/2022 13 180 OK MW-24A Mercury 7/19/2022 7/27/2022 8 180 OK MW-24A Methyl Ethyl Ketone 7/19/2022 7/29/2022 10 14 OK MW-24A Methylene Chloride 7/19/2022 7/29/2022 10 14 OK MW-24A Molybdenum 7/19/2022 8/1/2022 13 180 OK MW-24A Naphthalene 7/19/2022 7/29/2022 10 14 OK MW-24A Nickel 7/19/2022 8/1/2022 13 180 OK MW-24A Nitrate + Nitrite as N 7/19/2022 7/29/2022 10 28 OK MW-24A Nitrogen, Ammonia as N 7/19/2022 7/26/2022 7 28 OK MW-24A Potassium 7/19/2022 8/3/2022 15 180 OK MW-24A Selenium 7/19/2022 8/1/2022 13 180 OK MW-24A Silver 7/19/2022 8/1/2022 13 180 OK MW-24A Sodium 7/19/2022 8/11/2022 23 180 OK MW-24A Sulfate 7/19/2022 7/22/2022 3 28 OK MW-24A Tetrahydrofuran 7/19/2022 7/29/2022 10 14 OK MW-24A Thallium 7/19/2022 8/1/2022 13 180 OK MW-24A Tin 7/19/2022 8/3/2022 15 180 OK MW-24A Toluene 7/19/2022 7/29/2022 10 14 OK MW-24A Total Dissolved Solids 7/19/2022 7/22/2022 3 7 OK MW-24A Uranium 7/19/2022 8/1/2022 13 180 OK MW-24A Vanadium 7/19/2022 8/1/2022 13 180 OK MW-24A Xylenes, total 7/19/2022 7/29/2022 10 14 OK MW-24A Zinc 7/19/2022 8/1/2022 13 180 OK MW-25 Acetone 7/13/2022 7/18/2022 5 14 OK MW-25 Arsenic 7/13/2022 7/29/2022 16 180 OK MW-25 Benzene 7/13/2022 7/18/2022 5 14 OK MW-25 Beryllium 7/13/2022 7/29/2022 16 180 OK MW-25 Bicarbonate as CaCO3 7/13/2022 7/19/2022 6 14 OK MW-25 Cadmium 7/13/2022 7/29/2022 16 180 OK MW-25 Calcium 7/13/2022 7/28/2022 15 180 OK MW-25 Carbon Tetrachloride 7/13/2022 7/18/2022 5 14 OK MW-25 Carbonate as CO3 7/13/2022 7/19/2022 6 14 OK MW-25 Chloride 7/13/2022 7/16/2022 3 28 OK MW-25 Chloroform 7/13/2022 7/18/2022 5 14 OK MW-25 Chloromethane 7/13/2022 7/18/2022 5 14 OK MW-25 Chromium 7/13/2022 7/29/2022 16 180 OK MW-25 Cobalt 7/13/2022 7/29/2022 16 180 OK MW-25 Copper 7/13/2022 7/29/2022 16 180 OK MW-25 Fluoride 7/13/2022 7/16/2022 3 28 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-25 Gross Radium Alpha 7/13/2022 8/19/2022 37 180 OK MW-25 Iron 7/13/2022 7/28/2022 15 180 OK MW-25 Lead 7/13/2022 7/29/2022 16 180 OK MW-25 Magnesium 7/13/2022 7/28/2022 15 180 OK MW-25 Manganese 7/13/2022 7/29/2022 16 180 OK MW-25 Mercury 7/13/2022 7/21/2022 8 180 OK MW-25 Methyl Ethyl Ketone 7/13/2022 7/18/2022 5 14 OK MW-25 Methylene Chloride 7/13/2022 7/18/2022 5 14 OK MW-25 Molybdenum 7/13/2022 7/29/2022 16 180 OK MW-25 Naphthalene 7/13/2022 7/18/2022 5 14 OK MW-25 Nickel 7/13/2022 7/29/2022 16 180 OK MW-25 Nitrate + Nitrite as N 7/13/2022 7/26/2022 13 28 OK MW-25 Nitrogen, Ammonia as N 7/13/2022 7/26/2022 13 28 OK MW-25 Potassium 7/13/2022 7/28/2022 15 180 OK MW-25 Selenium 7/13/2022 7/29/2022 16 180 OK MW-25 Silver 7/13/2022 7/29/2022 16 180 OK MW-25 Sodium 7/13/2022 7/28/2022 15 180 OK MW-25 Sulfate 7/13/2022 8/1/2022 19 28 OK MW-25 Tetrahydrofuran 7/13/2022 7/18/2022 5 14 OK MW-25 Thallium 7/13/2022 7/29/2022 16 180 OK MW-25 Tin 7/13/2022 7/28/2022 15 180 OK MW-25 Toluene 7/13/2022 7/18/2022 5 14 OK MW-25 Total Dissolved Solids 7/13/2022 7/18/2022 5 7 OK MW-25 Uranium 7/13/2022 7/29/2022 16 180 OK MW-25 Vanadium 7/13/2022 7/29/2022 16 180 OK MW-25 Xylenes, total 7/13/2022 7/18/2022 5 14 OK MW-25 Zinc 7/13/2022 7/29/2022 16 180 OK MW-26 Acetone 7/14/2022 7/18/2022 4 14 OK MW-26 Arsenic 7/14/2022 7/29/2022 15 180 OK MW-26 Benzene 7/14/2022 7/18/2022 4 14 OK MW-26 Beryllium 7/14/2022 7/29/2022 15 180 OK MW-26 Bicarbonate as CaCO3 7/14/2022 7/20/2022 6 14 OK MW-26 Cadmium 7/14/2022 7/29/2022 15 180 OK MW-26 Calcium 7/14/2022 7/28/2022 14 180 OK MW-26 Carbon Tetrachloride 7/14/2022 7/18/2022 4 14 OK MW-26 Carbonate as CO3 7/14/2022 7/20/2022 6 14 OK MW-26 Chloride 7/14/2022 7/19/2022 5 28 OK MW-26 Chloroform 7/14/2022 7/18/2022 4 14 OK MW-26 Chloromethane 7/14/2022 7/18/2022 4 14 OK MW-26 Chromium 7/14/2022 7/29/2022 15 180 OK MW-26 Cobalt 7/14/2022 7/29/2022 15 180 OK MW-26 Copper 7/14/2022 7/29/2022 15 180 OK MW-26 Fluoride 7/14/2022 7/19/2022 5 28 OK MW-26 Gross Radium Alpha 7/14/2022 8/17/2022 34 180 OK MW-26 Iron 7/14/2022 7/28/2022 14 180 OK MW-26 Lead 7/14/2022 7/29/2022 15 180 OK MW-26 Magnesium 7/14/2022 7/28/2022 14 180 OK MW-26 Manganese 7/14/2022 7/29/2022 15 180 OK MW-26 Mercury 7/14/2022 7/21/2022 7 180 OK MW-26 Methyl Ethyl Ketone 7/14/2022 7/18/2022 4 14 OK MW-26 Methylene Chloride 7/14/2022 7/18/2022 4 14 OK MW-26 Molybdenum 7/14/2022 7/29/2022 15 180 OK MW-26 Naphthalene 7/14/2022 7/18/2022 4 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-26 Nickel 7/14/2022 7/29/2022 15 180 OK MW-26 Nitrate + Nitrite as N 7/14/2022 7/26/2022 12 28 OK MW-26 Nitrogen, Ammonia as N 7/14/2022 7/26/2022 12 28 OK MW-26 Potassium 7/14/2022 7/28/2022 14 180 OK MW-26 Selenium 7/14/2022 7/29/2022 15 180 OK MW-26 Silver 7/14/2022 7/29/2022 15 180 OK MW-26 Sodium 7/14/2022 7/28/2022 14 180 OK MW-26 Sulfate 7/14/2022 7/19/2022 5 28 OK MW-26 Tetrahydrofuran 7/14/2022 7/18/2022 4 14 OK MW-26 Thallium 7/14/2022 7/29/2022 15 180 OK MW-26 Tin 7/14/2022 7/28/2022 14 180 OK MW-26 Toluene 7/14/2022 7/18/2022 4 14 OK MW-26 Total Dissolved Solids 7/14/2022 7/18/2022 4 7 OK MW-26 Uranium 7/14/2022 7/29/2022 15 180 OK MW-26 Vanadium 7/14/2022 7/29/2022 15 180 OK MW-26 Xylenes, total 7/14/2022 7/18/2022 4 14 OK MW-26 Zinc 7/14/2022 7/29/2022 15 180 OK MW-27 Fluoride 7/15/2022 7/22/2022 7 28 OK MW-27 Nitrate + Nitrite as N 7/15/2022 8/2/2022 18 28 OK MW-28 Chloride 7/15/2022 8/12/2022 28 28 OK MW-28 Nitrate+ Nitrite as N 7/15/2022 8/2/2022 18 28 OK MW-28 Selenium 7/15/2022 8/1/2022 17 180 OK MW-28 Uranium 7/15/2022 8/1/2022 17 180 OK MW-29 Uranium 7/14/2022 8/1/2022 18 180 OK MW-30 Acetone 7/13/2022 7/18/2022 5 14 OK MW-30 Arsenic 7/13/2022 7/29/2022 16 180 OK MW-30 Benzene 7/13/2022 7/18/2022 5 14 OK MW-30 Beryllium 7/13/2022 7/29/2022 16 180 OK MW-30 Bicarbonate as CaCO3 7/13/2022 7/19/2022 6 14 OK MW-30 Cadmium 7/13/2022 7/29/2022 16 180 OK MW-30 Calcium 7/13/2022 7/28/2022 15 180 OK MW-30 Carbon Tetrachloride 7/13/2022 7/18/2022 5 14 OK MW-30 Carbonate as CO3 7/13/2022 7/19/2022 6 14 OK MW-30 Chloride 7/13/2022 7/16/2022 3 28 OK MW-30 Chloroform 7/13/2022 7/18/2022 5 14 OK MW-30 Chloromethane 7/13/2022 7/18/2022 5 14 OK MW-30 Chromium 7/13/2022 7/29/2022 16 180 OK MW-30 Cobalt 7/13/2022 7/29/2022 16 180 OK MW-30 Copper 7/13/2022 7/29/2022 16 180 OK MW-30 Fluoride 7/13/2022 7/16/2022 3 28 OK MW-30 Gross Radium Alpha 7/13/2022 8/17/2022 35 180 OK MW-30 Iron 7/13/2022 7/28/2022 15 180 OK MW-30 Lead 7/13/2022 7/29/2022 16 180 OK MW-30 Magnesium 7/13/2022 7/28/2022 15 180 OK MW-30 Manganese 7/13/2022 7/29/2022 16 180 OK MW-30 Mercury 7/13/2022 7/21/2022 8 180 OK MW-30 Methyl Ethyl Ketone 7/13/2022 7/18/2022 5 14 OK MW-30 Methylene Chloride 7/13/2022 7/18/2022 5 14 OK MW-30 Molybdenum 7/13/2022 7/29/2022 16 180 OK MW-30 Naphthalene 7/13/2022 7/18/2022 5 14 OK MW-30 Nickel 7/13/2022 7/29/2022 16 180 OK MW-30 Nitrate+ Nitrite as N 7/13/2022 7/27/2022 14 28 OK MW-30 Nitrogen, Ammonia as N 7/13/2022 7/26/2022 13 28 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analvsis Date (Days) Time (Days) Check MW-30 Potassium 7/13/2022 7/28/2022 15 180 OK MW-30 Selenium 7/13/2022 7/29/2022 16 180 OK MW-30 Silver 7/13/2022 7/29/2022 16 180 OK MW-30 Sodium 7/13/2022 7/28/2022 15 180 OK MW-30 Sulfate 7/13/2022 8/1/2022 19 28 OK MW-30 Tetrahydrofuran 7/13/2022 7/18/2022 5 14 OK MW-30 Thallium 7/13/2022 7/29/2022 16 180 OK MW-30 Tin 7/13/2022 7/28/2022 15 180 OK MW-30 Toluene 7/13/2022 7/18/2022 5 14 OK MW-30 Total Dissolved Solids 7/13/2022 7/18/2022 5 7 OK MW-30 Uranium 7/13/2022 7/29/2022 16 180 OK MW-30 Vanadium 7/13/2022 7/29/2022 16 180 OK MW-30 Xylenes, total 7/13/2022 7/18/2022 5 14 OK MW-30 Zinc 7/13/2022 7/29/2022 16 180 OK MW-31 Acetone 7/12/2022 7/18/2022 6 14 OK MW-31 Arsenic 7/12/2022 7/29/2022 17 180 OK MW-31 Benzene 7/12/2022 7/18/2022 6 14 OK MW-31 Beryllium 7/12/2022 7/29/2022 17 180 OK MW-31 Bicarbonate as CaCO3 7/12/2022 7/19/2022 7 14 OK MW-31 Cadmium 7/12/2022 7/29/2022 17 180 OK MW-31 Calcium 7/12/2022 7/28/2022 16 180 OK MW-31 Carbon Tetrachloride 7/12/2022 7/18/2022 6 14 OK MW-31 Carbonate as CO3 7/12/2022 7/19/2022 7 14 OK MW-31 Chloride 7/12/2022 8/1/2022 20 28 OK MW-31 Chloroform 7/12/2022 7/18/2022 6 14 OK MW-31 Chloromethane 7/12/2022 7/18/2022 6 14 OK MW-31 Chromium 7/12/2022 7/29/2022 17 180 OK MW-31 Cobalt 7/12/2022 7/29/2022 17 180 OK MW-31 Copper 7/12/2022 7/29/2022 17 180 OK MW-31 Fluoride 7/12/2022 7/16/2022 4 28 OK MW-31 Gross Radium Alpha 7/12/2022 8/17/2022 36 180 OK MW-31 Iron 7/12/2022 7/28/2022 16 180 OK MW-31 Lead 7/12/2022 7/29/2022 17 180 OK MW-31 Magnesium 7/12/2022 7/28/2022 16 180 OK MW-31 Manganese 7/12/2022 7/29/2022 17 180 OK MW-31 Mercury 7/12/2022 7/21/2022 9 180 OK MW-31 Methyl Ethyl Ketone 7/12/2022 7/18/2022 6 14 OK MW-31 Methylene Chloride 7/12/2022 7/18/2022 6 14 OK MW-31 Molybdenum 7/12/2022 7/29/2022 17 180 OK MW-31 Naphthalene 7/12/2022 7/18/2022 6 14 OK MW-31 Nickel 7/12/2022 7/29/2022 17 180 OK MW-31 Nitrate + Nitrite as N 7/12/2022 7/18/2022 6 28 OK MW-31 Nitrogen, Ammonia as N 7/12/2022 7/26/2022 14 28 OK MW-31 Potassium 7/12/2022 7/28/2022 16 180 OK MW-31 Selenium 7/12/2022 7/29/2022 17 180 OK MW-31 Silver 7/12/2022 7/29/2022 17 180 OK MW-31 Sodium 7/12/2022 7/28/2022 16 180 OK MW-31 Sulfate 7/12/2022 8/1/2022 20 28 OK MW-31 Tetrahydrofuran 7/12/2022 7/18/2022 6 14 OK MW-31 Thallium 7/12/2022 7/29/2022 17 180 OK MW-31 Tin 7/12/2022 7/28/2022 16 180 OK MW-31 Toluene 7/12/2022 7/18/2022 6 14 OK MW-31 Total Dissolved Solids 7/12/2022 7/18/2022 6 7 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Davs) Time (Days) Check MW-31 Uranium 7/12/2022 7/29/2022 17 180 OK MW-31 Vanadium 7/12/2022 7/29/2022 17 180 OK MW-31 Xylenes, total 7/12/2022 7/18/2022 6 14 OK MW-31 Zinc 7/12/2022 7/29/2022 17 180 OK MW-32 Chloride 7/15/2022 7/22/2022 7 28 OK MW-36 Acetone 7/13/2022 7/18/2022 5 14 OK MW-36 Arsenic 7/13/2022 7/29/2022 16 180 OK MW-36 Benzene 7/13/2022 7/18/2022 5 14 OK MW-36 Beryllium 7/13/2022 7/29/2022 16 180 OK MW-36 Bicarbonate as CaCO3 7/13/2022 7/20/2022 7 14 OK MW-36 Cadmium 7/13/2022 7/29/2022 16 180 OK MW-36 Calcium 7/13/2022 7/28/2022 15 180 OK MW-36 Carbon Tetrachloride 7/13/2022 7/18/2022 5 14 OK MW-36 Carbonate as CO3 7/13/2022 7/20/2022 7 14 OK MW-36 Chloride 7/13/2022 7/16/2022 3 28 OK MW-36 Chloroform 7/13/2022 7/18/2022 5 14 OK MW-36 Chloromethane 7/13/2022 7/18/2022 5 14 OK MW-36 Chromium 7/13/2022 7/29/2022 16 180 OK MW-36 Cobalt 7/13/2022 7/29/2022 16 180 OK MW-36 Copper 7/13/2022 7/29/2022 16 180 OK MW-36 Fluoride 7/13/2022 7/16/2022 3 28 OK MW-36 Gross Radium Alpha 7/13/2022 8/17/2022 35 180 OK MW-36 Iron 7/13/2022 7/28/2022 15 180 OK MW-36 Lead 7/13/2022 7/29/2022 16 180 OK MW-36 Magnesium 7/13/2022 7/28/2022 15 180 OK MW-36 Manganese 7/13/2022 7/29/2022 16 180 OK MW-36 Mercury 7/13/2022 7/21/2022 8 180 OK MW-36 Methyl Ethyl Ketone 7/13/2022 7/18/2022 5 14 OK MW-36 Methylene Chloride 7/13/2022 7/18/2022 5 14 OK MW-36 Molybdenum 7/13/2022 7/29/2022 16 180 OK MW-36 Naphthalene 7/13/2022 7/18/2022 5 14 OK MW-36 Nickel 7/13/2022 7/29/2022 16 180 OK MW-36 Nitrate+ Nitrite as N 7/13/2022 7/26/2022 13 28 OK MW-36 Nitrogen, Ammonia as N 7/13/2022 7/26/2022 13 28 OK MW-36 Potassium 7/13/2022 7/28/2022 15 180 OK MW-36 Selenium 7/13/2022 7/29/2022 16 180 OK MW-36 Silver 7/13/2022 7/29/2022 16 180 OK MW-36 Sodium 7/13/2022 7/28/2022 15 180 OK MW-36 Sulfate 7/13/2022 8/1/2022 19 28 OK MW-36 Tetrahydrofuran 7/13/2022 7/18/2022 5 14 OK MW-36 Thallium 7/13/2022 7/29/2022 16 180 OK MW-36 Tin 7/13/2022 7/28/2022 15 180 OK MW-36 Toluene 7/13/2022 7/18/2022 5 14 OK MW-36 Total Dissolved Solids 7/13/2022 7/18/2022 5 7 OK MW-36 Uranium 7/13/2022 7/29/2022 16 180 OK MW-36 Vanadium 7/13/2022 7/29/2022 16 180 OK MW-36 Xylenes. total 7/13/2022 7/18/2022 5 14 OK MW-36 Zinc 7/13/2022 7/29/2022 16 180 OK MW-38 Acetone 7/20/2022 7/29/2022 9 14 OK MW-38 Arsenic 7/20/2022 8/1/2022 12 180 OK MW-38 Benzene 7/20/2022 7/29/2022 9 14 OK MW-38 Beryllium 7/20/2022 8/1/2022 12 180 OK MW-38 Bicarbonate as CaCO3 7/20/2022 7/21/2022 1 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-38 Cadmium 7/20/2022 8/1/2022 12 180 OK MW-38 Calcium 7/20/2022 8/3/2022 14 180 OK MW-38 Carbon Tetrachloride 7/20/2022 7/29/2022 9 14 OK MW-38 Carbonate as CO3 7/20/2022 7/21/2022 I 14 OK MW-38 Chloride 7/20/2022 7/22/2022 2 28 OK MW-38 Chloroform 7/20/2022 7/29/2022 9 14 OK MW-38 Chloromethane 7/20/2022 7/29/2022 9 14 OK MW-38 Chromium 7/20/2022 8/1/2022 12 180 OK MW-38 Cobalt 7/20/2022 8/1/2022 12 180 OK MW-38 Copper 7/20/2022 8/1/2022 12 180 OK MW-38 Fluoride 7/20/2022 7/22/2022 2 28 OK MW-38 Gross Radium Alpha 7/20/2022 8/17/2022 28 180 OK MW-38 Iron 7/20/2022 8/3/2022 14 180 OK MW-38 Lead 7/20/2022 8/1/2022 12 180 OK MW-38 Magnesium 7/20/2022 8/3/2022 14 180 OK MW-38 Manganese 7/20/2022 8/1/2022 12 180 OK MW-38 Mercury 7/20/2022 7/27/2022 7 180 OK MW-38 Methyl Ethyl Ketone 7/20/2022 7/29/2022 9 14 OK MW-38 Methylene Chloride 7/20/2022 7/29/2022 9 14 OK MW-38 Molybdenum 7/20/2022 8/1/2022 12 180 OK MW-38 Naphthalene 7/20/2022 7/29/2022 9 14 OK MW-38 Nickel 7/20/2022 8/1/2022 12 180 OK MW-38 Nitrate+ Nitrite as N 7/20/2022 8/2/2022 13 28 OK MW-38 Nitrogen, Ammonia as N 7/20/2022 7/26/2022 6 28 OK MW-38 Potassium 7/20/2022 8/3/2022 14 180 OK MW-38 Selenium 7/20/2022 8/1/2022 12 180 OK MW-38 Silver 7/20/2022 8/1/2022 12 180 OK MW-38 Sodium 7/20/2022 8/3/2022 14 180 OK MW-38 Sulfate 7/20/2022 7/22/2022 2 28 OK MW-38 Tetrahydrofuran 7/20/2022 7/29/2022 9 14 OK MW-38 Thallium 7/20/2022 8/1/2022 12 180 OK MW-38 Tin 7/20/2022 8/3/2022 14 180 OK MW-38 Toluene 7/20/2022 7/29/2022 9 14 OK MW-38 Total Dissolved Solids 7/20/2022 7/22/2022 2 7 OK MW-38 Uranium 7/20/2022 8/1/2022 12 180 OK MW-38 Vanadium 7/20/2022 8/1/2022 12 180 OK MW-38 Xylenes, total 7/20/2022 7/29/2022 9 14 OK MW-38 Zinc 7/20/2022 8/1/2022 12 180 OK MW-39 Acetone 7/14/2022 7/18/2022 4 14 OK MW-39 Arsenic 7/14/2022 7/29/2022 15 180 OK MW-39 Benzene 7/14/2022 7/18/2022 4 14 OK MW-39 Beryllium 7/14/2022 7/29/2022 15 180 OK MW-39 Bicarbonate as CaCO3 7/14/2022 7/20/2022 6 14 OK MW-39 Cadmium 7/14/2022 7/29/2022 15 180 OK MW-39 Calcium 7/14/2022 7/28/2022 14 180 OK MW-39 Carbon Tetrachloride 7/14/2022 7/18/2022 4 14 OK MW-39 Carbonate as CO3 7/14/2022 7/20/2022 6 14 OK MW-39 Chloride 7/14/2022 7/18/2022 4 28 OK MW-39 Chloroform 7/14/2022 7/18/2022 4 14 OK MW-39 Chloromethane 7/14/2022 7/18/2022 4 14 OK MW-39 Chromium 7/14/2022 7/29/2022 15 180 OK MW-39 Cobalt 7/14/2022 7/29/2022 15 180 OK MW-39 Copper 7/14/2022 7/29/2022 15 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analvsis Date (Days) Time (Days) Check MW-39 Fluoride 7/14/2022 7/18/2022 4 28 OK MW-39 Gross Radium Alpha 7/14/2022 8/17/2022 34 180 OK MW-39 Iron 7/14/2022 7/28/2022 14 180 OK MW-39 Lead 7/14/2022 7/29/2022 15 180 OK MW-39 Magnesium 7/14/2022 7/28/2022 14 180 OK MW-39 Manganese 7/14/2022 7/29/2022 15 180 OK MW-39 Mercury 7/14/2022 7/21/2022 7 180 OK MW-39 Methyl Ethyl Ketone 7/14/2022 7/18/2022 4 14 OK MW-39 Methylene Chloride 7/14/2022 7/18/2022 4 14 OK MW-39 Molybdenum 7/14/2022 7/29/2022 15 180 OK MW-39 Naphthalene 7/14/2022 7/18/2022 4 14 OK MW-39 Nickel 7/14/2022 7/29/2022 15 180 OK MW-39 Nitrate + Nitrite as N 7/14/2022 7/26/2022 12 28 OK MW-39 Nitrogen, Ammonia as N 7/14/2022 7/26/2022 12 28 OK MW-39 Potassium 7/14/2022 7/28/2022 14 180 OK MW-39 Selenium 7/14/2022 7/29/2022 15 180 OK MW-39 Silver 7/14/2022 7/29/2022 15 180 OK MW-39 Sodium 7/14/2022 7/28/2022 14 180 OK MW-39 Sulfate 7/14/2022 7/19/2022 5 28 OK MW-39 Tetrahydrofuran 7/14/2022 7/18/2022 4 14 OK MW-39 Thallium 7/14/2022 7/29/2022 15 180 OK MW-39 Tin 7/14/2022 7/28/2022 14 180 OK MW-39 Toluene 7/14/2022 7/18/2022 4 14 OK MW-39 Total Dissolved Solids 7/14/2022 7/18/2022 4 7 OK MW-39 Uranium 7/14/2022 7/29/2022 15 180 OK MW-39 Vanadium 7/14/2022 7/29/2022 15 180 OK MW-39 Xylenes, total 7/14/2022 7/18/2022 4 14 OK MW-39 Zinc 7/14/2022 7/29/2022 15 180 OK MW-40 Acetone 7/14/2022 7/18/2022 4 14 OK MW-40 Arsenic 7/14/2022 7/29/2022 15 180 OK MW-40 Benzene 7/14/2022 7/18/2022 4 14 OK MW-40 Beryllium 7/14/2022 7/29/2022 15 180 OK MW-40 Bicarbonate as CaCO3 7/14/2022 7/20/2022 6 14 OK MW-40 Cadmium 7/14/2022 7/29/2022 15 180 OK MW-40 Calcium 7/14/2022 7/28/2022 14 180 OK MW-40 Carbon Tetrachloride 7/14/2022 7/18/2022 4 14 OK MW-40 Carbonate as CO3 7/14/2022 7/20/2022 6 14 OK MW-40 Chloride 7/14/2022 7/18/2022 4 28 OK MW-40 Chloroform 7/14/2022 7/18/2022 4 14 OK MW-40 Chloromethane 7/14/2022 7/18/2022 4 14 OK MW-40 Chromium 7/14/2022 7/29/2022 15 180 OK MW-40 Cobalt 7/14/2022 7/29/2022 15 180 OK MW-40 Copper 7/14/2022 7/29/2022 15 180 OK MW-40 Fluoride 7/14/2022 7/18/2022 4 28 OK MW-40 Gross Radium Alpha 7/14/2022 8/17/2022 34 180 OK MW-40 Iron 7/14/2022 7/28/2022 14 180 OK MW-40 Lead 7/14/2022 7/29/2022 15 180 OK MW-40 Magnesium 7/14/2022 7/28/2022 14 180 OK MW-40 Manganese 7/14/2022 7/29/2022 15 180 OK MW-40 Mercury 7/14/2022 7/21/2022 7 180 OK MW-40 Methyl Ethyl Ketone 7/14/2022 7/18/2022 4 14 OK MW-40 Methylene Chloride 7/14/2022 7/18/2022 4 14 OK MW-40 Molybdenum 7/14/2022 7/29/2022 15 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-40 Naphthalene 7/14/2022 7/18/2022 4 14 OK MW-40 Nickel 7/14/2022 7/29/2022 15 180 OK MW-40 Nitrate+ Nitrite as N 7/14/2022 7/26/2022 12 28 OK MW-40 Nitrogen, Ammonia as N 7/14/2022 7/26/2022 12 28 OK MW-40 Potassium 7/14/2022 7/28/2022 14 180 OK MW-40 Selenium 7/14/2022 7/29/2022 15 180 OK MW-40 Silver 7/14/2022 7/29/2022 15 180 OK MW-40 Sodium 7/14/2022 8/1/2022 18 180 OK MW-40 Sulfate 7/14/2022 7/19/2022 5 28 OK MW-40 Tetrahydrofuran 7/14/2022 7/18/2022 4 14 OK MW-40 Thallium 7/14/2022 7/29/2022 15 180 OK MW-40 Tin 7/14/2022 7/28/2022 14 180 OK MW-40 Toluene 7/14/2022 7/18/2022 4 14 OK MW-40 Total Dissolved Solids 7/14/2022 7/18/2022 4 7 OK MW-40 Uranium 7/14/2022 7/29/2022 15 180 OK MW-40 Vanadium 7/14/2022 7/29/2022 15 180 OK MW-40 Xylenes, total 7/14/2022 7/18/2022 4 14 OK MW-40 Zinc 7/14/2022 7/29/2022 15 180 OK MW-65 Acetone 7/20/2022 7/29/2022 9 14 OK MW-65 Arsenic 7/20/2022 8/1/2022 12 180 OK MW-65 Benzene 7/20/2022 7/29/2022 9 14 OK MW-65 Beryllium 7/20/2022 8/1/2022 12 180 OK MW-65 Bicarbonate as CaCO3 7/20/2022 7/21/2022 I 14 OK MW-65 Cadmium 7/20/2022 8/1/2022 12 180 OK MW-65 Calcium 7/20/2022 8/3/2022 14 180 OK MW-65 Carbon Tetrachloride 7/20/2022 7/29/2022 9 14 OK MW-65 Carbonate as CO3 7/20/2022 7/21/2022 I 14 OK MW-65 Chloride 7/20/2022 7/22/2022 2 28 OK MW-65 Chloroform 7/20/2022 7/29/2022 9 14 OK MW-65 Chloromethane 7/20/2022 7/29/2022 9 14 OK MW-65 Chromium 7/20/2022 8/1/2022 12 180 OK MW-65 Cobalt 7/20/2022 8/1/2022 12 180 OK MW-65 Copper 7/20/2022 8/1/2022 12 180 OK MW-65 Fluoride 7/20/2022 7/22/2022 2 28 OK MW-65 Gross Radium Alpha 7/20/2022 8/17/2022 28 180 OK MW-65 Iron 7/20/2022 8/3/2022 14 180 OK MW-65 Lead 7/20/2022 8/1/2022 12 180 OK MW-65 Magnesium 7/20/2022 8/3/2022 14 180 OK MW-65 Manganese 7/20/2022 8/1/2022 12 180 OK MW-65 Mercury 7/20/2022 7/27/2022 7 180 OK MW-65 Methyl Ethyl Ketone 7/20/2022 7/29/2022 9 14 OK MW-65 Methylene Chloride 7/20/2022 7/29/2022 9 14 OK MW-65 Molybdenum 7/20/2022 8/1/2022 12 180 OK MW-65 Naphthalene 7/20/2022 7/29/2022 9 14 OK MW-65 Nickel 7/20/2022 8/1/2022 12 180 OK MW-65 Nitrate+ Nitrite as N 7/20/2022 8/2/2022 13 28 OK MW-65 Nitrogen, Ammonia as N 7/20/2022 7/26/2022 6 28 OK MW-65 Potassium 7/20/2022 8/3/2022 14 180 OK MW-65 Selenium 7/20/2022 8/1/2022 12 180 OK MW-65 Silver 7/20/2022 8/1/2022 12 180 OK MW-65 Sodium 7/20/2022 8/3/2022 14 180 OK MW-65 Sulfate 7/20/2022 7/26/2022 6 28 OK MW-65 Tetrahydrofuran 7/20/2022 7/29/2022 9 14 OK G-2A: Quarterly Holding Time Evaluation HQl.d Time Allowed Hold fiold Time Location ID Parameler Name Saml)le Date Analysis Date (Days) Tiine (Days) Check MW-65 Thallium 7/20/2022 8/1/2022 12 180 OK MW-65 Tin 7/20/2022 8/3/2022 14 180 OK MW-65 Toluene 7/20/2022 7/29/2022 9 14 OK MW-65 Total Dissolved Solids 7/20/2022 7/22/2022 2 7 OK MW-65 Uranium 7/20/2022 8/1/2022 12 180 OK MW-65 Vanadium 7/20/2022 8/1/2022 12 180 OK MW-65 Xylenes, total 7/20/2022 7/29/2022 9 14 OK MW-65 Zinc 7/20/2022 8/1/2022 12 180 OK G-2B: Accelerated Holding Time Evaluation Allowed Hold Time Hold Time Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) (Days) Check Trip Blank Chloroform 8/9/2022 8/12/2022 3 14 OK Trip Blank Chloroform 9/22/2022 9/30/2022 8 14 OK MW-11 Sulfate 8/8/2022 8/31/2022 23 28 OK MW-11 Chloride 8/8/2022 8/17/2022 9 28 OK MW-11 Manganese 8/8/2022 8/19/2022 11 180 OK MW-11 Nitrate + Nitrite as N 8/8/2022 8/16/2022 8 28 OK MW-11 Total Dissolved Solids 8/8/2022 8/12/2022 4 7 OK MW-11 Sulfate 9/21/2022 10/4/2022 13 28 OK MW-11 Chloride 9/21/2022 10/1/2022 10 28 OK MW-1 I Manganese 9/21/2022 9/29/2022 8 180 OK MW-11 Nitrate+ Nitrite as N 9/21/2022 9/23/2022 2 28 OK MW-11 Total Dissolved Solids 9/21/2022 9/28/2022 7 7 OK MW-25 Total Dissolved Solids 8/9/2022 8/12/2022 3 7 OK MW-25 Total Dissolved Solids 9/20/2022 9/27/2022 7 7 OK MW-26 Chloride 8/9/2022 8/19/2022 10 28 OK MW-26 Chloroform 8/9/2022 8/12/2022 3 14 OK MW-26 Nitrate + Nitrite as N 8/9/2022 8/16/2022 7 28 OK MW-26 Total Dissolved Solids 8/9/2022 8/12/2022 3 7 OK MW-26 Chloride 9/20/2022 10/1/2022 11 28 OK MW-26 Chloroform 9/20/2022 9/30/2022 IO 14 OK MW-26 Nitrate + Nitrite as N 9/20/2022 9/23/2022 3 28 OK MW-30 Chloride 8/9/2022 8/19/2022 10 28 OK MW-30 Uranium 8/9/2022 8/19/2022 10 180 OK MW-30 Selenium 8/9/2022 8/19/2022 10 180 OK MW-30 Nitrate+ Nitrite as N 8/9/2022 8/17/2022 8 28 OK MW-30 Total Dissolved Solids 8/9/2022 8/12/2022 3 7 OK MW-30 Chloride 9/20/2022 10/5/2022 15 28 OK MW-30 Uranium 9/20/2022 9/29/2022 9 180 OK MW-30 Selenium 9/20/2022 9/29/2022 9 180 OK MW-30 Nitrate + Nitrite as N 9/20/2022 9/23/2022 3 28 OK MW-31 Sulfate 8/8/2022 8/31/2022 23 28 OK MW-31 Chloride 8/8/2022 8/17/2022 9 28 OK MW-31 Uranium 8/8/2022 8/19/2022 11 180 OK MW-31 Nitrate+ Nitrite as N 8/8/2022 8/17/2022 9 28 OK MW-31 Total Dissolved Solids 8/8/2022 8/12/2022 4 7 OK MW-31 Sulfate 9/20/2022 10/4/2022 14 28 OK MW-31 Chloride 9/20/2022 10/5/2022 15 28 OK MW-31 Uranium 9/20/2022 9/29/2022 9 180 OK MW-31 Nitrate + Nitrite as N 9/20/2022 9/23/2022 3 28 OK MW-31 Total Dissolved Solids 9/20/2022 9/27/2022 7 7 OK MW-65 Chloride 8/9/2022 8/20/2022 11 28 OK MW-65 Uranium 8/9/2022 8/19/2022 10 180 OK MW-65 Selenium 8/9/2022 8/19/2022 IO 180 OK MW-65 Nitrate+ Nitrite as N 8/9/2022 8/17/2022 8 28 OK MW-65 Total Dissolved Solids 8/9/2022 8/12/2022 3 7 OK MW-65 Total Dissolved Solids 9/20/2022 9/27/2022 7 7 OK G-3A: Quarterly Sample Laboratory Receipt Temperature CheckSample Batch WeUs in Batcb Temperature GEL 587184 MW-ll,MW-14,MW-24A,MW-25,MW-26,MW-30,MW-NA 31,MW-36,MW-38,MW-39,MW-40,MW-65 GEL587833 MW-24 Resample NA CTF22G1280 MW-11,MW-14,MW-25,MW-26,MW-30,MW-31,MW-1.1 oc 36, MW-39, MW-40, Trip Blank CTF 2201743 MW-12, MW-24, MW-24A, MW-27, MW-28, MW-29, MW-0.1 °C 32, MW-38, MW-65, Trip Blank NIA= These shipments contained samples for the analysis of gross alpha or metals only. Per Table 1 in the approved QAP, samples submitted for gross alpha or metals analyses do not have a sample temperature requirement. G-3B: Accelerated Sample Laboratory Receipt Temperature Check Sample Batch Wells in Batch Temperature CTF 22Hl255 -August MW-11, MW-25, MW-26, MW-30, MW-31, MW-65, Trip -0.3 °CBlank CTF 22F0888 -September MW-11, MW-25, MW-26, MW-30, MW-31, MW-65, Trip -0.3 °CBlank G-4A: Quarterly Sample Analytical Method Check Parameter QAPMethod Method tlsed by Lab Ammonia (as N) A4500-NH3 G or E350.l E350.l Nitrate+ Nitrite (as N) E353.1 or E353.2 E353.2 Metals E200.7 or E200.8 E200.7 and E200.8 Gross Alpha E900.0 or E900. l or E903.0 E903.0 voes SW8260B or SW8260C or SW8260D SW8260D Chloride A4500-Cl B or A4500-Cl E or E300.0 SM4500-Cl-E and 300.0 Fluoride A4500-F C or E300.0 E300.0 Sulfate A4500-SO4 E or E300.0 E300.0 TDS A2540 C A2540 C Carbonate as CO3, Bicarbonate as HCO3 A2320 B A2320B Mercury E245. l or E200.7 or E200.8 E245.1 Calcium, Magnesium, Potassium, Sodium E200.7 E200.7 G-4B: Accelerated Sample Analytical Method Check Paramehir QAPMethod Method U�ed by Lab Nitrate+ Nitrite (as N) E353.l or E353.2 E353.2 Metals E200.7 or E200.8 E200.7 or E200.8 voes SW8260B or SW8260C or SW8260D SW8260C and SW8260D Chloride A4500-Cl B or A4500-Cl E or E300.0 E300.0 Sulfate A4500-SO4 E or E300.0 E300.0 TDS A2540 C A2540 C GSAQ -1 S uartcny 1 R ampe eportmg 11mt ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check Trip Blank Acetone 20 ug/L u I 20 OK Trip Blank Benzene I ug/L u I I OK Trip Blank Carbon Tetrachloride I ug/L u I 1 OK Trip Blank Chloroform I ug/L u I I OK Trip Blank Chloromethane I ug/L u I I OK Trip Blank Methyl Ethyl Ketone 20 ug/L u I 20 OK Trip Blank Methylene Chloride 1 ug/L u I I OK Trip Blank Naphthalene I ug/L u I l OKTrip Blank Tetrahydrofuran I ug/L u I I OK Trip Blank Toluene 1 ug/L u 1 I OK Trip Blank Xylenes, total I ug/L u 1 I OK Trip Blank Acetone 20 ug/L u I 20 OK Trip Blank Benzene 1 ug/L u 1 1 OK Trip Blank Carbon Tetrachloride 1 ug/L u l I OK Trip Blank Chloroform I ug/L u I 1 OK Trip Blank Chloromethane l ug/L u 1 1 OK Trip Blank Methyl Ethyl Ketone 20 ug/L u I 20 OK Trip Blank Methylene Chloride I ug/L u I I OK Trip Blank Naphthalene 1 ug/L u J I OK Trip Blank Tetrahydrofuran l ug/L u I I OK Trip Blank Toluene I ug/L u 1 l OK Trip Blank Xylenes, total 1 ug/L u I 1 OK MW-11 Acetone 20 ug/L u I 20 OK MW-11 Arsenic 5 ug/L u I 5 OK MW-11 Benzene l ug/L u I I OK MW-11 Beryllium 0.5 ug/L u I 0.5 OK MW-11 Bicarbonate as CaCO3 I rng/L I 1 OK MW-11 Cadmium 0.5 ug/L u I 0.5 OK MW-11 Calcium 0.2 mg/L I 0.5 OK MW-II Carbon Tetrachloride I ug/L u I I OK MW-11 Carbonate as CO3 1 mg/L u 1 I OK MW-11 Chloride I mg/L 1 I OK MW-11 Chloroform I ug/L u 1 I OK MW-11 Chloromethane 1 ug/L u I 1 OK MW-11 Chromium 25 ug/L u I 25 OK MW-11 Cobalt 10 ug/L u I JO OK MW-11 Copper 10 ug/L u I 10 OK MW-11 Fluoride 0.1 mg/L I 0.1 OK MW-11 Gross Radium Alpha 0.861 pCi/L u I 1 OK MW-11 Iron 30 ug/L u 1 30 OK MW-11 Lead I ug/L u 1 I OK MW-11 Magnesium 0.2 mg/L I 0.5 OK MW-11 Manganese 10 ug/L 1 10 OK MW-11 Mercury 0.5 ug/L u 1 0.5 OK MW-11 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-II Methylene Chloride I ug/L u 1 I OK MW-11 Molybdenum 10 ug/L u I 10 OK MW-11 Naphthalene I ug/L u 1 I OK MW-11 Nickel 20 ug/L u 1 20 OK MW-11 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-11 Nitrogen, Ammonia as N 0.25 mg/L 5 0.05 OK MW-11 Potassium 0.5 mg/L I 0.5 OK MW-11 Selenium 5 ug/L I 5 OK MW-11 Silver 10 ug/L u 1 10 OK G-5A Quarterly Sample Reporting Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-11 Sodium 0.5 mg/L 1 0.5 OK MW-11 Sulfate 20 mg/L 20 l OKMW-11 Tetrahydrofuran I ug/L u 1 I OK MW-11 Thallium 0.5 ug/L u 1 0.5 OK MW-11 Tin 100 ug/L u 1 JOO OK MW-11 Toluene I ug/L u 1 1 OK MW-11 Total Dissolved Solids 20 MG/L 2 10 OK MW-11 Uranium 0.3 ug/L I 0.3 OK MW-11 Vanadium 15 ug/L u 1 15 OK MW-11 Xylenes, total 1 ug/L u 1 I OK MW-I I Zinc 10 ug/L u 1 10 OK MW-12 Selenium 5 ug/L 1 5 OK MW-12 Uranium 0.3 ug/L I 0.3 OK MW-14 Acetone 20 ug/L u 1 20 OK MW-14 Arsenic 5 ug/L u 1 5 OK MW-14 Benzene 1 ug/L u 1 I OK MW-14 Beryllium 0.5 ug/L u 1 0.5 OK MW-14 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-14 Cadmium 0.5 ug/L 1 0.5 OK MW-14 Calcium 0.2 mg/L 1 0.5 OK MW-14 Carbon Tetrachloride I ug/L u 1 1 OK MW-14 Carbonate as CO3 1 mg/L u 1 I OK MW-14 Chloride I mg/L I I OK MW-14 Chloroform 1 ug/L u I 1 OK MW-14 Chloromethane 1 ug/L u 1 1 OK MW-14 Chromium 25 ug/L u I 25 OK MW-14 Cobalt 10 ug/L u I IO OK MW-14 Cooner 10 ug/L u I 10 OK MW-14 Fluoride 0.1 mg/L u l 0.1 OK MW-14 Gross Radium Alpha 0.949 pCi/L u l 1 OK MW-14 Iron 30 ug/L u 1 30 OK MW-14 Lead I ug/L u 1 1 OK MW-14 Magnesium 0.2 mg/L 1 0.5 OK MW-14 Manganese 10 ug/L 1 10 OK MW-14 Mercury 0.5 ug/L u 1 0.5 OK MW-14 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-14 Methylene Chloride I ug/L u 1 I OK MW-14 Molybdenum 10 ug/L u I 10 OK MW-14 Naphthalene I ug/L u I 1 OK MW-14 Nickel 20 ug/L u 1 20 OK MW-14 Nitrate + Nitrite as N 0.1 mg/L u 1 0.1 OK MW-14 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-14 Potassium 0.5 mg/L 1 0.5 OK MW-14 Selenium 5 ug/L u 1 5 OK MW-14 Silver IO ug/L u 1 10 OK MW-14 Sodium 0.5 mg/L 1 0.5 OK MW-14 Sulfate 50 mg/L 50 1 OK MW-14 Tetrahydrofuran 1 ug/L u 1 1 OK MW-14 Thallium 0.5 ug/L u 1 0.5 OK MW-14 Tin 100 ug/L u 1 100 OK MW-14 Toluene 1 ug/L u 1 l OK MW-14 Total Dissolved Solids 20 MG/L 2 10 OK MW-14 Uranium 0.3 ug/L 1 0.3 OK MW-14 Vanadium 15 ug/L u I 15 OK G-5A Quarterly Sample Reporting Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-14 Xylenes, total 1 ug/L u 1 1 OK MW-14 Zinc 10 ug/L 1 10 OK MW-24 Acetone 20 ug/L u l 20 OK MW-24 Arsenic 5 ug/L u l 5 OK MW-24 Benzene I ug/L u l 1 OK MW-24 Beryllium 0.5 ug/L 1 0.5 OK MW-24 Bicarbonate as CaCO3 I mg/L u I I OK MW-24 Cadmium 0.5 ug/L l 0.5 OK MW-24 Calcium 2 mg/L 10 0.5 OK MW-24 Carbon Tetrachloride I ug/L u l l OK MW-24 Carbonate as CO3 I mg/L u I 1 OK MW-24 Chloride 1 mg/L 1 1 OK MW-24 Chloroform l ug/L u 1 1 OK MW-24 Chloromethane I ug/L u 1 l OK MW-24 Chromium 25 ug/L u I 25 OK MW-24 Cobalt 10 ug/L 1 10 OK MW-24 Copper 10 ug/L I 10 OK MW-24 Fluoride 0.1 mg/L 1 0.1 OK MW-24 Iron 30 ug/L u 1 30 OK MW-24 Lead I ug/L I I OK MW-24 Magnesium 0.2 mg/L I 0.5 OK MW-24 Manganese 25 ug/L 50 10 OK MW-24 Mercury 0.5 ug/L u I 0.5 OK MW-24 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-24 Methylene Chloride I ug/L u 1 I OK MW-24 Molybdenum 10 ug/L u I 10 OK MW-24 Naphthalene I ug/L u 1 1 OK MW-24 Nickel 20 ug/L I 20 OK MW-24 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-24 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-24 Potassium 0.5 mg/L 1 0.5 OK MW-24 Selenium 5 ug/L I 5 OK MW-24 Silver 10 ug/L u 1 10 OK MW-24 Sodium 5 mg/L 10 0.5 OK MW-24 Sulfate 100 mg/L 100 1 OK MW-24 Tetrahydrofuran 1 ug/L u 1 1 OK MW-24 Thallium 0.5 ug/L I 0.5 OK MW-24 Tin 100 ug/L u I 100 OK MW-24 Toluene 1 ug/L u 1 1 OK MW-24 Total Dissolved Solids 20 MG/L 2 10 OK MW-24 Uranium 0.3 ug/L 1 0.3 OK MW-24 Vanadium 15 ug/L u 1 15 OK MW-24 Xylenes, total 1 ug/L u 1 1 OK MW-24 Zinc 10 ug/L I 10 OK MW-24 Gross Radium Alpha 0.782 pCi/L l 1 OK MW-24A Acetone 20 ug/L u 1 20 OK MW-24A Arsenic 5 ug/L u I 5 OK MW-24A Benzene 1 ug/L u l I OK MW-24A Beryllium 0.5 ug/L 1 0.5 OK MW-24A Bicarbonate as CaCO3 1 mg/L u 1 1 OK MW-24A Cadmium 0.5 ug/L 1 0.5 OK MW-24A Calcium 2 mg/L 10 0.5 OK MW-24A Carbon Tetrachloride I ug/L u 1 I OK MW-24A Carbonate as CO3 1 mg/L u 1 I OK G-5A Quarterly Sample Reportin_g Limit Check Lab Required Reporting Dilution Reporting RL Location Analvte Limit Units Qualifier Factor Limit Check MW-24A Chloride 1 mg/L I 1 OK MW-24A Chloroform 1 ug/L u I I OK MW-24A Chloromethane I ug/L u l 1 OK MW-24A Chromium 25 ug/L u I 25 OK MW-24A Cobalt 10 ug/L 1 10 OK MW-24A Copper IO ug/L 1 IO OK MW-24A Fluoride 0.1 mg/L 1 0.1 OK MW-24A Gross Radium Alpha 0.981 pCi/L I 1 OK MW-24A Iron 30 ug/L u I 30 OK MW-24A Lead 1 ug/L u I I OK MW-24A Magnesium 0.2 mg/L 1 0.5 OK MW-24A Manganese 25 ug/L 50 10 OK MW-24A Mercury 0.5 ug/L u 1 0.5 OK MW-24A Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-24A Methylene Chloride 1 ug/L u 1 1 OK MW-24A Molybdenum 10 ug/L u 1 10 OK MW-24A Naphthalene I ug/L u 1 1 OK MW-24A Nickel 20 ug/L I 20 OK MW-24A Nitrate + Nitrite as N 0.1 mg/L I 0.1 OK MW-24A Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-24A Potassium 0.5 mg/L 1 0.5 OK MW-24A Selenium 5 ug/L 1 5 OK MW-24A Silver 10 ug/L u I 10 OK MW-24A Sodium 5 mg/L 10 0.5 OK MW-24A Sulfate 100 mg/L 100 1 OK MW-24A Tetrahydrofuran 1 ug/L u 1 1 OK MW-24A Thallium 0.5 ug/L 1 0.5 OK MW-24A Tin 100 ug/L u I 100 OK MW-24A Toluene 1 ug/L u 1 1 OK MW-24A Total Dissolved Solids 20 MG/L 2 10 OK MW-24A Uranium 0.3 ug/L I 0.3 OK MW-24A Vanadium 15 ug/L u I 15 OK MW-24A Xylenes, total I ug/L u 1 1 OK MW-24A Zinc 10 ug/L I 10 OK MW-25 Acetone 20 ug/L u I 20 OK MW-25 Arsenic 5 ug/L u I 5 OK MW-25 Benzene I ug/L u I 1 OK MW-25 Beryllium 0.5 ug/L u I 0.5 OK MW-25 Bicarbonate as CaCO3 1 mg/L I 1 OK MW-25 Cadmium 0.5 ug/L 1 0.5 OK MW-25 Calcium 0.2 mg/L 1 0.5 OK MW-25 Carbon Tetrachloride 1 ug/L u 1 I OK MW-25 Carbonate as CO3 I mg/L u 1 I OK MW-25 Chloride 1 mg/L 1 1 OK MW-25 Chloroform 1 ug/L u I 1 OK MW-25 Chloromethane I ug/L u 1 1 OK MW-25 Chromium 25 ug/L u I 25 OK MW-25 Cobalt 10 ug/L u 1 10 OK MW-25 Copper 10 ug/L u 1 10 OK MW-25 Fluoride 0.1 mg/L 1 0.1 OK MW-25 Gross Radium Alpha 0.915 pCi/L u I 1 OK MW-25 Iron 30 ug/L u I 30 OK MW-25 Lead I ug/L u 1 I OK MW-25 Magnesium 0.2 mg/L I 0.5 OK G5AQ -uaner1y amp c . l S I R epornng 1m1t ec L" . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-25 Manganese JO ug/L I 10 OK MW-25 Mercury 0.5 ug/L u I 0.5 OK MW-25 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-25 Methylene Chloride 1 ug/L u I 1 OK MW-25 Molybdenum 10 ug/L 1 10 OK MW-25 Naphthalene 1 ug/L u 1 1 OK MW-25 Nickel 20 ug/L u 1 20 OK MW-25 Nitrate+ Nitrite as N 0.1 mg/L u 1 0.1 OK MW-25 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-25 Potassium 0.5 mg/L 1 0.5 OK MW-25 Selenium 5 ug/L u 1 5 OK MW-25 Silver 10 ug/L u 1 10 OK MW-25 Sodium 0.5 mg/L 1 0.5 OK MW-25 Sulfate 20 mg/L 20 1 OK MW-25 Tetrahydrofuran l ug/L u 1 1 OK MW-25 Thallium 0.5 ug/L 1 0.5 OK MW-25 Tin 100 ug/L u 1 100 OK MW-25 Toluene I ug/L u 1 1 OK MW-25 Total Dissolved Solids 20 MG/L 2 10 OK MW-25 Uranium 0.3 ug/L 1 0.3 OK MW-25 Vanadium 15 ug/L u I 15 OK MW-25 Xylenes, total I ug/L u 1 1 OK MW-25 Zinc 10 ug/L u 1 10 OK MW-26 Acetone 20 ug/L u l 20 OK MW-26 Arsenic 5 ug/L u I 5 OK MW-26 Benzene 1 ug/L u I 1 OK MW-26 Beryllium 0.5 ug/L u I 0.5 OK MW-26 Bicarbonate as CaCO3 l mg/L I 1 OK MW-26 Cadmium 0.5 ug/L 1 0.5 OK MW-26 Calcium 0.2 mg/L 1 0.5 OK MW-26 Carbon Tetrachloride l ug/L u 1 I OK MW-26 Carbonate as CO3 l mg/L u I I OK MW-26 Chloride I mg/L I I OK MW-26 Chloroform I ug/L u 1 1 OK MW-26 Chloromethane l ug/L u 1 I OK MW-26 Chromium 25 ug/L u I 25 OK MW-26 Cobalt 10 ug/L u 1 10 OK MW-26 Copper 10 ug/L u 1 10 OK MW-26 Fluoride 0.1 mg/L 1 0.1 OK MW-26 Gross Radium Alpha 0.952 pCi/L 1 I OK MW-26 Iron 30 ug/L u l 30 OK MW-26 Lead 1 ug/L u 1 1 OK MW-26 Magnesium 0.2 mg/L 1 0.5 OK MW-26 Manganese 10 ug/L 1 10 OK MW-26 Mercury 0.5 ug/L u 1 0.5 OK MW-26 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-26 Methylene Chloride l ug/L u I 1 OK MW-26 Molybdenum 10 ug/L u 1 10 OK MW-26 Naphthalene 1 ug/L u 1 1 OK MW-26 Nickel 20 ug/L u 1 20 OK MW-26 Nitrate+ Nitrite as N 0.1 m_g/L l 0.1 OK MW-26 Nitrogen, Ammonia as N 0.05 mg/L l 0.05 OK MW-26 Potassium 0.5 mg/L 1 0.5 OK MW-26 Selenium 5 ug/L 1 5 OK G-5A Quarterly Sample Reporting Limit Check Lab Required Reporting Dilution Reporting RL Location Analvte Limit Units Qualifier Factor Limit Check MW-26 Silver 10 ug/L u 1 10 OK MW-26 Sodium 0.5 mg/L 1 0.5 OK MW-26 Sulfate 50 mg/L 50 1 OK MW-26 Tetrahydrofuran 1 ug/L u 1 1 OK MW-26 Thallium 0.5 ug/L u 1 0.5 OK MW-26 Tin 100 ug/L u 1 100 OK MW-26 Toluene I ug/L u I 1 OK MW-26 Total Dissolved Solids 20 MG/L 2 10 OK MW-26 Uranium 0.3 ug/L 1 0.3 OK MW-26 Vanadium 15 ug/L u 1 15 OK MW-26 X vlenes, total I ug/L u 1 1 OK MW-26 Zinc 10 ug/L u I 10 OK MW-27 Fluoride 0.1 mg/L I 0.1 OK MW-27 Nitrate+ Nitrite as N 0.5 mg/L 5 0.1 OK MW-28 Chloride JO mg/L 10 1 OK MW-28 Nitrate+ Nitrite as N 0.5 mg/L 5 0.1 OK MW-28 Selenium 5 ug/L 1 5 OK MW-28 Uranium 0.3 ug/L 1 0.3 OK MW-29 Uranium 0.3 ug/L 1 0.3 OK MW-30 Acetone 20 ug/L u 1 20 OK MW-30 Arsenic 5 ug/L u 1 5 OK MW-30 Benzene 1 ug/L u 1 I OK MW-30 Beryllium 0.5 ug/L u 1 0.5 OK MW-30 Bicarbonate as CaCO3 1 mg/L I I OK MW-30 Cadmium 0.5 ug/L u I 0.5 OK MW-30 Calcium 0.2 mg/L I 0.5 OK MW-30 Carbon Tetrachloride l ug/L u 1 l OK MW-30 Carbonate as CO3 l mg/L u l I OK MW-30 Chloride 20 mg/L 20 1 OK MW-30 Chloroform 1 ug/L u 1 1 OK MW-30 Chloromethane 1 ug/L u l 1 OK MW-30 Chromium 25 ug/L u 1 25 OK MW-30 Cobalt 10 ug/L u 1 10 OK MW-30 Coooer 10 ug/L u I 10 OK MW-30 Fluoride 0.1 mg/L 1 0.1 OK MW-30 Gross Radium Alpha 0.973 pCi/L u l 1 OK MW-30 Iron 30 ug/L u 1 30 OK MW-30 Lead 1 ug/L u 1 I OK MW-30 Magnesium 0.2 mg/L 1 0.5 OK MW-30 Manganese 10 ug/L u 1 10 OK MW-30 Mercury 0.5 ug/L u I 0.5 OK MW-30 Methyl Ethyl Ketone 20 ug/L u l 20 OK MW-30 Methylene Chloride 1 ug/L u 1 l OK MW-30 Molybdenum 10 ug/L u 1 10 OK MW-30 Naphthalene 1 ug/L u 1 1 OK MW-30 Nickel 20 ug/L u 1 20 OK MW-30 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-30 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-30 Potassium 0.5 mg/L 1 0.5 OK MW-30 Selenium 5 ug/L 1 5 OK MW-30 Silver 10 ug/L u 1 10 OK MW-30 Sodium 0.5 mg/L 1 0.5 OK MW-30 Sulfate 10 mg/L 10 1 OK MW-30 Tetrahvdrofuran 1 ug/L u 1 1 OK Location MW-30 MW-30 MW-30 MW-30 MW-30 MW-30 MW-30 MW-30 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-31 MW-32 MW-36 MW-36 GSAQ -uarter1y amp1e I S I R Analyte Thallium Tin Toluene Total Dissolved Solids Uranium Vanadium Xylenes, total Zinc Acetone Arsenic Benzene Beryllium Bicarbonate as CaCO3 Cadmium Calcium Carbon Tetrachloride Carbonate as CO3 Chloride Chloroform Chloromethane Chromium Cobalt Coooer Fluoride Gross Radium Alpha Iron Lead Magnesium Manganese Mercury Methyl Ethyl Ketone Methylene Chloride Molybdenum Naphthalene Nickel Nitrate + Nitrite as N Nitrogen, Ammonia as N Potassium Selenium Silver Sodium Sulfate Tetrahydrofuran Thallium Tin Toluene Total Dissolved Solids Uranium Vanadium Xylenes, total Zinc Chloride Acetone Arsenic epor11n_g 1m1t ec L" -Ch k Lab Required Reporting Dilution Reporting RL Limit Units Qualifier Factor Limit Check 0.5 ug/L u 1 0.5 OK 100 ug/L u I 100 OK 1 ug/L u l 1 OK 20 MG/L 2 10 OK 0.3 ug/L 1 0.3 OK 15 ug/L u 1 15 OK 1 ug/L u 1 1 OK 10 ug/L u 1 10 OK 20 u_g/L u 1 20 OK 5 ug/L u 1 5 OK 1 ug/L u 1 1 OK 0.5 ug/L u 1 0.5 OK I mg/L 1 1 OK 0.5 ug/L u 1 0.5 OK 0.2 mg/L 1 0.5 OK 1 ug/L u 1 1 OK 1 mg/L u 1 1 OK 5 m_g/L 5 1 OK 1 u_g/L u 1 1 OK l ug/L u 1 I OK 25 ug/L u 1 25 OK IO u_g/L u I 10 OK 10 u_g/L u l 10 OK 0.1 mg/L 1 0.1 OK 1.01 pCi/L I I OK 30 u_g/L u I 30 OK 1 u_g/L u l 1 OK 0.2 mg/L 1 0.5 OK 10 ug/L u 1 10 OK 0.5 ug/L u 1 0.5 OK 20 u_g/L u I 20 OK 1 ug/L u 1 1 OK 10 ug/L u I 10 OK 1 ug/L u I I OK 20 u_g/L u 1 20 OK 1 m_g/L 10 0.1 OK 0.05 mg/L 1 0.05 OK 0.5 mg/L l 0.5 OK 5 ug/L I 5 OK 10 u_g/L u 1 IO OK 0.5 m_g/L l 0.5 OK 20 m_g/L 20 1 OK 1 ug/L u 1 I OK 0.5 ug/L u 1 0.5 OK 100 ug/L u 1 100 OK I u_g/L u 1 1 OK 20 MG/L 2 10 OK 0.3 ug/L 1 0.3 OK 15 ug/L u 1 15 OK 1 ug/L u 1 1 OK 10 u_g/L u 1 10 OK 1 mf!/L 1 l OK 20 ug/L u 1 20 OK 5 ug/L u 1 5 OK G-5A Quarterly Sample Reporting Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-36 Benzene I ug/L u I 1 OK MW-36 Beryllium 0.5 ug/L u I 0.5 OK MW-36 Bicarbonate as CaCO3 I mg/L l 1 OK MW-36 Cadmium 0.5 ug/L u 1 0.5 OK MW-36 Calcium 0.2 mg/L 1 0.5 OK MW-36 Carbon Tetrachloride 1 ug/L u I 1 OK MW-36 Carbonate as CO3 l mg/L u I 1 OK MW-36 Chloride l mg/L l I OK MW-36 Chloroform 1 ug/L u I 1 OK MW-36 Chloromethane 1 ug/L u I 1 OK MW-36 Chromium 25 ug/L u I 25 OK MW-36 Cobalt 10 ug/L u I 10 OK MW-36 Copper 10 ug/L u 1 10 OK MW-36 Fluoride 0.1 mg/L I 0.1 OK MW-36 Gross Radium Alpha 0.91 pCi/L u I 1 OK MW-36 Iron 30 ug/L u .I 30 OK MW-36 Lead l ug/L u I I OK MW-36 Magnesium 0.2 mg/L 1 0.5 OK MW-36 Manganese 10 ug/L u I 10 OK MW-36 Mercury 0.5 ug/L u 1 0.5 OK MW-36 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-36 Methylene Chloride I ug/L u I l OK MW-36 Molybdenum JO ug/L u 1 10 OK MW-36 Naphthalene I ug/L u 1 1 OK MW-36 Nickel 20 ug/L u 1 20 OK MW-36 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-36 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-36 Potassium 0.5 mg/L 1 0.5 OK MW-36 Selenium 5 ug/L I 5 OK MW-36 Silver 10 ug/L u I 10 OK MW-36 Sodium 5 mg/L JO 0.5 OK MW-36 Sulfate 50 mg/L 50 I OK MW-36 Tetrahydrofuran I ug/L u 1 l OK MW-36 Thallium 0.5 ug/L 1 0.5 OK MW-36 Tin JOO ug/L u 1 100 OK MW-36 Toluene 1 ug/L u 1 1 OK MW-36 Total Dissolved Solids 20 MG/L 2 10 OK MW-36 Uranium 0.3 ug/L I 0.3 OK MW-36 Vanadium 15 ug/L u 1 15 OK MW-36 Xylenes, total I ug/L u 1 1 OK MW-36 Zinc 10 ug/L u 1 10 OK MW-38 Acetone 20 ug/L u J 20 OK MW-38 Arsenic 5 ug/L u 1 5 OK MW-38 Benzene 1 ug/L u 1 1 OK MW-38 Beryllium 0.5 ug/L u I 0.5 OK MW-38 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-38 Cadmium 0.5 ug/L u 1 0.5 OK MW-38 Calcium 0.2 mg/L 1 0.5 OK MW-38 Carbon Tetrachloride 1 ug/L u 1 l OK MW-38 Carbonate as CO3 1 mg/L u I 1 OK MW-38 Chloride 1 mg/L l l OK MW-38 Chloroform l ug/L u 1 I OK MW-38 Chloromethane l ug/L u 1 I OK MW-38 Chromium 25 ug/L u 1 25 OK G-5A Quarterly Sample Reporting Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-38 Cobalt 10 ug/L u 1 10 OK MW-38 Cooner IO ug/L u I 10 OK MW-38 Fluoride 0.1 mg/L I 0.1 OK MW-38 Gross Radium Alpha 0.928 pCi/L u I 1 OK MW-38 Iron 30 ug/L u 1 30 OK MW-38 Lead 1 ug/L u I 1 OK MW-38 Magnesium 0.2 mg/L I 0.5 OK MW-38 Manganese 10 ug/L u 1 10 OK MW-38 Mercury 0.5 ug/L u 1 0.5 OK MW-38 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-38 Methylene Chloride I ug/L u 1 I OK MW-38 Molybdenum 10 ug/L u I 10 OK MW-38 Naphthalene I ug/L u 1 I OK MW-38 Nickel 20 ug/L u 1 20 OK MW-38 Nitrate+ Nitrite as N I mg/L 10 0.1 OK MW-38 Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-38 Potassium 0.5 mg/L I 0.5 OK MW-38 Selenium 5 ug/L I 5 OK MW-38 Silver 10 ug/L u I 10 OK MW-38 Sodium 0.5 mg/L I 0.5 OK MW-38 Sulfate 100 mg/L 100 I OK MW-38 Tetrahydrofuran 1 ug/L u I I OK MW-38 Thallium 0.5 ug/L u I 0.5 OK MW-38 Tin 100 ug/L u I 100 OK MW-38 Toluene 1 ug/L u 1 I OK MW-38 Total Dissolved Solids 20 MG/L 2 10 OK MW-38 Uranium 0.3 ug/L I 0.3 OK MW-38 Vanadium 15 ug/L u 1 15 OK MW-38 Xylenes, total I ug/L u 1 I OK MW-38 Zinc 10 ug/L u I 10 OK MW-39 Acetone 20 ug/L u l 20 OK MW-39 Arsenic 5 ug/L u I 5 OK MW-39 Benzene I ug/L u 1 1 OK MW-39 Beryllium 0.5 ug/L 1 0.5 OK MW-39 Bicarbonate as CaCO3 I m_g/L u 1 1 OK MW-39 Cadmium 0.5 ug/L 1 0.5 OK MW-39 Calcium 0.2 mg/L I 0.5 OK MW-39 Carbon Tetrachloride I ug/L u 1 1 OK MW-39 Carbonate as CO3 1 mg/L u I 1 OK MW-39 Chloride I mg/L 1 1 OK MW-39 Chloroform I ug/L u I 1 OK MW-39 Chloromethane 1 u_g/L u 1 1 OK MW-39 Chromium 25 ug/L u 1 25 OK MW-39 Cobalt 10 ug/L 1 10 OK MW-39 Copper 10 ug/L I 10 OK MW-39 Fluoride 0.1 mg/L I 0.1 OK MW-39 Gross Radium Alpha 0.904 pCi/L I 1 OK MW-39 Iron 30 ug/L 1 30 OK MW-39 Lead 1 ug/L u 1 1 OK MW-39 Magnesium 0.2 mg/L 1 0.5 OK MW-39 Manganese 10 ug/L I 10 OK MW-39 Mercury 0.5 ug/L u I 0.5 OK MW-39 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-39 Methylene Chloride 1 ug/L u 1 1 OK G-5A Quanerly Sample Reporting Limit Check Lab Required Reporting Dilution Reporting RL Location -Analyte Limit Units Qualifier Factor Limit Check MW-39 Molybdenum 10 U,!!/L u I 10 OK MW-39 Naphthalene I ug/L u I 1 OK MW-39 Nickel 20 ug/L I 20 OK MW-39 Nitrate+ Nitrite as N 0.1 mg/L I 0.1 OK MW-39 Nitrogen, Ammonia as N 0.05 mg/L I 0.05 OK MW-39 Potassium 0.5 mg/L I 0.5 OK MW-39 Selenium 5 ug/L 1 5 OK MW-39 Silver IO ug/L u I 10 OK MW-39 Sodium 0.5 mg/L I 0.5 OK MW-39 Sulfate 50 mg/L 50 I OK MW-39 Tetrahydrofuran I ug/L u 1 1 OK MW-39 Thallium 0.5 ug/L I 0.5 OK MW-39 Tin 100 ug/L u 1 100 OK MW-39 Toluene 1 ug/L u 1 1 OK MW-39 Total Dissolved Solids 20 MOIL 2 10 OK MW-39 Uranium 0.3 ug/L 1 0.3 OK MW-39 Vanadium 15 ug/L u I 15 OK MW-39 Xylenes, total 1 ug/L u 1 I OK MW-39 Zinc JO ug/L I 10 OK MW-40 Acetone 20 ug/L u 1 20 OK MW-40 Arsenic 5 ug/L u I 5 OK MW-40 Benzene I ug/L u I I OK MW-40 Beryllium 0.5 ug/L u I 0.5 OK MW-40 Bicarbonate as CaCO3 I mg/L I 1 OK MW-40 Cadmium 0.5 ug/L u I 0.5 OK MW-40 Calcium 0.2 mg/L I 0.5 OK MW-40 Carbon Tetrachloride I ug/L u 1 I OK MW-40 Carbonate as CO3 1 mg/L u 1 1 OK MW-40 Chloride I mg/L 1 1 OK MW-40 Chloroform I ug/L u 1 1 OK MW-40 Chloromethane I ug/L u 1 I OK MW-40 Chromium 25 ug/L u l 25 OK MW-40 Cobalt IO ug/L u I 10 OK MW-40 Copper 10 ug/L u l 10 OK MW-40 Fluoride 0.1 mg/L I 0.1 OK MW-40 Gross Radium Alpha 0.899 pCi/L u I 1 OK MW-40 Iron 30 ug/L u I 30 OK MW-40 Lead I ug/L u 1 1 OK MW-40 Magnesium 0.2 mg/L I 0.5 OK MW-40 Manganese 10 ug/L 1 10 OK MW-40 Mercury 0.5 u_g/L u 1 0.5 OK MW-40 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-40 Methylene Chloride 1 ug/L u 1 I OK MW-40 Molybdenum 10 ug/L u 1 10 OK MW-40 Naphthalene 1 ug/L u 1 1 OK MW-40 Nickel 20 ug/L u 1 20 OK MW-40 Nitrate+ Nitrite as N 0.1 mg/L I 0.1 OK MW-40 Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-40 Potassium 0.5 mg/L 1 0.5 OK MW-40 Selenium 5 ug/L 1 5 OK MW-40 Silver 10 ug/L u 1 10 OK MW-40 Sodium 0.5 mg/L 1 0.5 OK MW-40 Sulfate 50 mg/L 50 I OK MW-40 Tetrahydrofuran 1 ug/L u I I OK G-5A Quarterly Sample Reporting Limit Check Lab Required Reporting Dilution Reporting RL Location Analvte Limit Units Qualifier Factor Limit Check MW-40 Thallium 0.5 ug/L u l 0.5 OK MW-40 Tin 100 ug/L u I 100 OK MW-40 Toluene 1 ug/L u 1 l OK MW-40 Total Dissolved Solids 20 MG/L 2 10 OK MW-40 Uranium 0.3 ug/L I 0.3 OK MW-40 Vanadium 15 ug/L u I 15 OK MW-40 Xylenes, total l ug/L u I l OK MW-40 Zinc 10 ug/L u I 10 OK MW-65 Acetone 20 ug/L u I 20 OK MW-65 Arsenic 5 ug/L u l 5 OK MW-65 Benzene l ug/L u I l OK MW-65 Beryllium 0.5 ug/L u I 0.5 OK MW-65 Bicarbonate as CaCO3 l mg/L I l OKMW-65 Cadmium 0.5 ug/L u I 0.5 OK MW-65 Calcium 0.2 mg/L l 0.5 OK MW-65 Carbon Tetrachloride J ug/L u I I OK MW-65 Carbonate as CO3 I mg/L u 1 I OKMW-65 Chloride I mg/L 1 I OK MW-65 Chloroform I ug/L u I I OK MW-65 Chloromethane I ug/L u I I OKMW-65 Chromium 25 ug/L u l 25 OKMW-65 Cobalt 10 ug/L u I 10 OK MW-65 Copper 10 ug/L u I 10 OK MW-65 Fluoride 0.1 mg/L I 0.1 OKMW-65 Gross Radium Alpha 0.884 pCi/L I I OKMW-65 Iron 30 ug/L u l 30 OK MW-65 Lead I ug/L u l I OK MW-65 Magnesium 0.2 mg/L I 0.5 OKMW-65 Manganese 10 ug/L u I 10 OKMW-65 Mercury 0.5 ug/L u I 0.5 OK MW-65 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-65 Methylene Chloride I ug/L u I I OKMW-65 Molybdenum 10 ug/L u I 10 OK MW-65 Naphthalene 1 ug/L u I I OK MW-65 Nickel 20 ug/L u l 20 OK MW-65 Nitrate+ Nitrite as N 1 mg/L 10 0.1 OKMW-65 Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-65 Potassium 0.5 mg/L 1 0.5 OK MW-65 Selenium 5 ug/L I 5 OKMW-65 Silver 10 ug/L u I 10 OK MW-65 Sodium 0.5 mg/L 1 0.5 OK MW-65 Sulfate 100 mg/L 100 I OKMW-65 Tetrahydrofuran 1 ug/L u 1 1 OK MW-65 Thallium 0.5 ug/L u I 0.5 OK MW-65 Tin 100 ug/L u 1 100 OKMW-65 Toluene I ug/L u 1 I OK MW-65 Total Dissolved Solids 20 MG/L 2 10 OK MW-65 Uranium 0.3 ug/L I 0.3 OK MW-65 Vanadium 15 ug/L u 1 15 OKMW-65 Xvlenes, total I ug/L u 1 1 OK MW-65 Zinc 10 ug/L u I 10 OK 0 SBA -cce erate ;:,,amp e d IR eporllng 1m1t ec L .. Ch k Lab Required Reporting Dilution Reporting Location Analyte i Limit Units Qualifier Factor Limit RLCheck Trip Blank Chloroform 1 uglL u 1 1 OK Trip Blank Chloroform 1 uglL u 1 1 OK MW-11 Sulfate 20 m_glL 20 1 OK MW-11 Chloride 1 mglL 1 1 OK MW-11 Manganese 10 uglL 1 10 OK MW-11 Nitrate+ Nitrite as N 0.1 mglL I 0.1 OK MW-11 Total Dissolved Solids 20 MGIL 2 10 OK MW-11 Sulfate 20 mglL 20 1 OK MW-11 Chloride 1 mglL I 1 OK MW-11 Manganese 10 uglL I 10 OK MW-11 Nitrate+ Nitrite as N 0.1 mglL I 0.1 OK MW-11 Total Dissolved Solids 20 MOIL 2 10 OK MW-25 Total Dissolved Solids 20 MOIL 2 10 OK MW-25 Total Dissolved Solids 20 MOIL 2 10 OK MW-26 Chloride l mg/L 1 I OK MW-26 Chloroform 100 uglL 100 I OK MW-26 Nitrate + Nitrite as N 0.1 mglL 1 0.1 OK MW-26 Total Dissolved Solids 20 MOIL 2 10 OK MW-26 Chloride 1 mglL I 1 OK MW-26 Chloroform 100 uglL 100 1 OK MW-26 Nitrate + Nitrite as N 0.1 mglL l 0.1 OK MW-30 Chloride 100 mglL 100 1 OK MW-30 Uranium 0.3 uglL 1 0.3 OK MW-30 Selenium 5 uglL 1 5 OK MW-30 Nitrate+ Nitrite as N 0.5 mg/L 5 0.1 OK MW-30 Total Dissolved Solids 20 MGIL 2 10 OK MW-30 Chloride 5 mglL 5 I OK MW-30 Uranium 0.3 uglL l 0.3 OK MW-30 Selenium 5 uglL I 5 OK MW-30 Nitrate+ Nitrite as N 0.5 mglL 5 0.1 OK MW-31 Sulfate 20 mg/L 20 1 OK MW-31 Chloride 1 mglL 1 1 OK MW-31 Uranium 0.3 uglL I 0.3 OK MW-31 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-31 Total Dissolved Solids 20 MG/L 2 10 OK MW-31 Sulfate 100 mglL 100 1 OK MW-31 Chloride 5 mg/L 5 1 OK MW-31 Uranium 0.3 uglL I 0.3 OK MW-31 Nitrate + Nitrite as N 0.5 mglL 5 0.1 OK MW-31 Total Dissolved Solids 20 MGIL 2 10 OK MW-65 Chloride 100 mglL 100 1 OK MW-65 Uranium 0.3 ug/L l 0.3 OK MW-65 Selenium 5 uglL l 5 OK MW-65 Nitrate+ Nitrite as N 0.5 mglL 5 0.1 OK MW-65 Total Dissolved Solids 20 MGIL 2 10 OK MW-65 Total Dissolved Solids 20 MOIL 2 10 OK G-6A: Quarterly Sample Trip Blank EvaluationLab Report Constituent Result 2-Butanone ND Acetone ND Benzene ND Carbon Tetrachloride ND Chloroform ND CTF 22Gl280 Chloromethane ND Methylene Chloride ND Naphthalene ND Tetrahydrofuran ND Toluene ND Xvlenes, Total ND 2-Butanone ND Acetone ND Benzene ND Carbon Tetrachloride ND Chloroform ND CTF 22Gl743 Chloromethane ND Methylene Chloride ND Naphthalene ND Tetrahydrofuran ND Toluene ND Xylenes, Total ND G-6B: Accelerated Sample Trip Blank EvaluationAll trip blanks for the Accelerated samples were non detect. Illank Sample Date Laboratory CTF 22H1255 -August 8/9/2022 CTF CTF 22F0888 -September 9/22/2022 CTF G-7 A: QA/QC Evaluation for Quarterly Sa mole Oupli.cates , onstituenl .MW-38 7/20122 MW-65 7 /20/22 %RPO Bicarbonate as CaCO3 (mg/L) 103 102 0.98 Calcium (mg/L) 461 509 9.90 Chloride (mg/L) 44.5 44.4 0.22 Fluoride (mg/L) 0.291 0.395 30.32 MaJ:?:nesium (mg/L) 190 206 8.08 Nitrate+ Nitrite (as N) (mg/L) 14.4 14.1 2.11 Potassium (mg/L) 26.6 27.0 1.49 Selenium (mg/L) 0.156 0.154 1.29 Sodium (mg/L) 387 386 0.26 Sulfate (mg/L) 2490 2480 0.40 TDS ( mJ:!:/L) 3910 3950 1.02 Uranium (mg/L) 0.0060 0.0060 0.00 Constituent G-8A: Quarterly Sample Radiologies Counting Error GY..O ,tp.b.a1 minus C.0'mrttingGn� s t\..lpha 1i:niuu Rn Bi ltn .and 'U P·ve • fon1 ID.t•J1or S 1,.-tfbin � u (:14-) 2()lo/iJ t;)Wtt (G\\.�CL? MW-11 l.00U 0.327 NC 3.75 NC MW-14 l.00U 0.246 NC 7.5 NC MW-24 2.55 0.449 y 7.5 NC MW-24A 3.56 0.653 y - MW-25 1.00 U 0.253 NC 7.5 NC MW-26 1.67 0.429 N 4.69 y MW-30 l.00U 0.973 NC 3.75 NC MW-31 1.22 0.412 N 7.5 y MW-36 l.00U 0.340 NC 7.5 NC MW-38 1.00U 0.304 NC - MW-39 2.04 0.475 N - MW-40 l.00U 0.280 NC - MW-65 1.14 0.354 NC - NIA -the counting error is less than 20% of the activity as required by the GWDP and this check column is not applicable. NC = Not calculated. The sample results are nondetect and the check is not applicable. G-8B: Radiologies Counting Error for Accelerated Samples There are no accelerated samples collected for Gross Alpha. 0-9A: Quarterly Sample Laboratory Matrix QC Matrix Spike % Recovery Comparison RPD Lab Report Well Analyte MS %REC MSD %REC REC Range RPD Range 2201280 MW-11 Calcium* NC NC 70 -130 2201280 MW-11 Sodium* NC NC 70 -130 2201280 MW-11 Sulfate 109 128 80 - I 20 2201280 MW-11 Chi oromethane 149 145 70 - 130 2201743 MW-24 Calcium* NC NC 70-130 2201743 MW-24 Magnesium* NC NC 70 -130 2201743 MW-24 Sodium* NC NC 70 -130 2201743 MW-38 Calcium* NC NC 70 -130 2201743 MW-38 Magnesium* NC NC 70 -130 2201743 MW-38 Sodium* NC NC 70 -130 2201743 MW-24 Manganese* NC **70 -130 2201743 MW-24 Sulfate* NC NC 80 - 120 2201743 MW-38 Sulfate* NC NC 80 -120 2201743 MW-38 Fluoride 63.7 64.5 80 - 120 2201743 MW-38 Fluoride 82.0 77.2 80 -120 2201743 MW-38 Nitrate 90.2 70.7 80 -120*Recovery was not calculated as the analyte level in the sample was greater than 4 times the spike amount. NA -QC was not performed on an EFRI sample. NC NC 2.37 3.06 NC NC NC NC NC NC ** NC NC 1.18 3.55 1.19 ** CTF routine QC does not include a MSD for metals analyzed by 200.8. Precision is determined by other QC samples as allowed by the analytical method. Method Blank Detections All Method Blanks for the quarter were non-detect. Laboratory Control Sample Lab Report Analyte LCS %REC REC Range 2201280 Acetone 141 70 -130 2201280 Choromethane 150 70 -130 2201743 Iron 117.0 85 -115 Laboratory Duplicate% Recovery Comparison Sample Result Lab Report Well Analyte (mg/L) Alkalinity (Carbonate 2201280 NA (CaC03)* NC *Recovery was not calculated due to the low analyte level in the sample. NA - QC was not performed on an EFRI sample. Surrogate % Recovery All surrogate recoveries for the quarter were within laboratory acceptance limits. Lab RPD Duplicate RPD% Range NC NC 10 20 20 20 20 20 20 20 20 20 20 ** 20 20 20 20 20 G-9B: Accelerated Laboratory Matrix QC Matrix pike % Recovery Comparison tab Repor-t -Well_ Analyte MS,%REC MSD %REC 22Hl255 -August Monthly MW-26 Chloroform* NC NC Carbon 22Hl255 -August Monthly MW-26 Tetrachloride 52.2 50.3 22Hl255 -August Monthly MW-26 Chloromethane 64.9 63.3 2212016 -September Monthly MW-11 Chloride 74.7 89.2 2212016 -September Monthly MW-11 Sulfate 68.6 60.6 2212016 -September Monthly NA Sulfate* NC NC 2212016 -September Monthly MW-26 Chloroform* NC NC *Recovery was not calculated as the analyte level in the sample was greater than 4 times the spike amount NA -QC was not performed on an EFRI sample. Laboratory Control Sample All Laboratory Control Samples were within acceptance limits for the quarter. Laboratory Duplicate % Recovery Comparison All Laboratory Duplicates were within acceptance limits for the quarter. Method Blank Detections All Method Blanks for the quarter were non-detect. Surrogate % Recovery All surrogate recoveries for the quarter were within laboratory acceptance limits. R:PDRange .RECRange .RPD o/o o/o 70-130 NC 20 70-130 3.71 20 70-130 2.50 20 80 -120 2.09 20 80 -120 1.120 20 80 -120 NC 20 70 -130 NC 20 TW4-43 �5523 TWN-20 [JS564 TW4-42 ¢5524 MW-38 �5463 estimated dry area temporary perched monitoring well installed September, 2021 showing elevation in feet amsl temporary perched nitrate monitoring well installed April, 2021 showing elevation in feet amsl temporary perched monitoring well installed April, 2019 showing elevation in feet amsl perched monitoring well installed February, 2018 showing elevation in feet amsl M;•;504 perched monitoring well showing elevation in feet amsl TW4-12 05568 temporary perched monitoring wellshowing elevation in feet amsl TWN-7 <>5569 temporary perched nitrate monitoringwell showing elevation in feet amsl PIEZ-1 perched piezometer showing '-5588 elevation in feet amsl RUIN SPRING c!, 5380 seep or spring showing elevation in feet amsl • . •· at 1 mile NOTE : MW-4, MW-26, TW4-1, TW4-2, TW4-4, TW4-11, , 4• , , , 4-4 an are c oro onn pumping we s; TW4-2.2. TW4-24, TW4-25 and TWN-2 are nitrate pumping wells; TW4-11 water level Is below the base of the Burro Canyon Fonnation HYDRO GEO CHEM, INC. KRIGED 3rd QUARTER, 2022 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE H:/718000/nov22/WUUwl0922.srf Time concentration plots for MW-01 Chloride in MW-01 60 -,-------------------------------, 50 --------------------------------1 40 +------------------------------ � 30 +.-------------------------------1 ·�:c ,.,., 0 -1-=----.-----.---�--�---�---.-----.---�---1 9,<:> \'&<:I 0.4 BINTERA Sample Date Fluoride in MW-01 ?,'o »"' ,,fl · .... �� Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values ■Non-Detected Values 5000 4500 4000 3500 ::;-3000 "bi; '; 2500 � 2000 1500 1000 500 --- BINTERA Time concentration plots for MW-01 -■ Sulfate in MW-01 ' ... -----� -- Sample Date Uranium in MW-01 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 .... - V -·-........ .,,._., •• Detected Values Non-Detected Values Time concentration plots for MW-02 Chloride in MW-02 80 ..---------------------------------, 70 +------------------------------1 60 +-------------------------------------1 so -·�--------------------------------1 GJ 40 +--------------------------------1 -� u 30 +-----1•-------------------------1 20 -HI�-----�-------------------------, 10 � _§.. 0.5 GJ "O Sample Date Fluoride in MW-02 ·:s 0.4 -------------------1---------------1 0.3 BINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values Time concentration plots for MW-02 Sulfate in MW-02 ::;- 1500 -1--111<&•----------------------------------l "iio .§. J!! J!! � 1000 -1-&--------------------------------l 14 ::i" 12 } E 10 ::, 'i: � 8 -INTERA Sample Date Uranium in MW-02 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values Time concentration plots for MW-03A Chloride in MW-03A _ 50 +----------+------------------------1 � .s cu 40 +--------------------------------1 "O ·.:: 0 6 30 +--------------------------------1 1.8 1.6 1.4 1.2 1 cu "O ·.::0.8 0 0.6 0.4 0.2 0 �" � § �,,,.;;. ..,-s l!!INTERA Sample Date Fluoride in MW-03A Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values Time concentration plots for MW-OJA Sulfate in MW-03A 4500 ..---------------------------------, 3500 3000 i 2500 2000 1500 1000 500 s:i" ...,_,<1' s:,'I �,,,--:.:. 40 35 30 _ 25 20 ·2 15 10 �%�NIE.:IA ,;;,°' �,,,<: Sample Date Uranium in MW-03A Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values Time concentration plots for MW-05 Chloride in MW-05 140 120 100 80 60 40 20 Sample Date Fluoride in MW-05 1.8 �-----------------------------, 1.6 ·------------------------------ 1.4 ------------------------------- 0.6 ------------------------------ 0.4 ------------------------------ 0.2 ------------------------------ Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 Detected Values Non-Detected Values Time concentration plots for MW-05 9000 8000 7000 6000 } 5000 4000 3000 2000 ·- I. 1000 0 160 140 120 _ 100 80 ·2 60 40 20 --0 ..-.cn5�NTERA Sulfate in MW-OS --.L -•-- Sample Date Uranium in MW-OS I -..... -•-- Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 -.... ,,,,.,,,,,__ ___" -• .. il/L_ •• Detected Values Non-Detected Values Time concentration plots for MW-11 Chloride in MW-11 80 -r------------------------------, 70 +----ff>------------------------------1 60 -t---a■t---------------------------- -50 � .§. ai 40 · "0 ·c u 30 20 -1--------------------------------1 10 ·t---------------------------------1 0 -1-----.------,---..----�------..-----..------.--------,-----1 ;J!'JINTERA Sample Date Fluoride in MW-11 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values 4.5 4 3.5 3 -= 2.5 ·2 2 1.5 1 0.5 ,;-:i:'b �'I> c.,"'� •INTERA Time concentration plots for MW-11 Sulfate in MW-11 Sample Date Uranium in MW-11 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values Time concentration plots for MW-12 Chloride in MW-12 160 ..-------------------------------, 140 -1------------------------------------l 120 +--_.-------------------------------1 _100 -1---------------------------------1 � .§. cu so 11----u-----------------------------1 :5! l:i :E u 60 20 ••l--------------------------------1 0 +---"""T""------r---,-------.------,----.------.----r-----t 0,4 0,35 0,3 _ 0.25 � .§. cu 0.2 "ti ·;:: i:i: 0.15 0.1 0.05 0 •INTERA Sample Date Fluoride in MW-12 '\ __J JI \J r\J- Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 ·�r � ' .J • 1 Detected Values Non-Detected Values 9000 8000 7000 6000 ] 5000 � 4000 3000 2000 1000 0 :>, � ""tt; c,"'� �,. 20 15 ·2 10 �¼�NIE.:IA Time concentration plots for MW-12 c:°'...,, �., Sulfate in MW-12 Sample Date Uranium in MW-12 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 Detected Values •Non-Detected Values 20 15 -� 10 l!!INTERA Time concentration plots for MW-14 Chloride in MW-14 Sample Date Fluoride in MW-14 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values Time concentration plots for MW-14 Sulfate in MW-14 0-1------.---�---�--�--�---------�-----1 ·2 ,X<o°' �o 80 60 40 BINTERA Sample Date Uranium in MW-14 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values ·;;: Time concentration plots for MW-15 Chloride in MW-15 40 30 20 0+--------.---�---------�--------_____j ,¥'b°' �o Sample Date Fluoride in MW-15 0.6 ..------------------------------� 0.5 ---------------------------------1 0.4 +---------------------------1---� 0.1 4----------------------------------J 0 +------r-----,---.....------.-----,---�--�----------J Sample Date e Detected Values �-¥s�NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •Non-Detected Values 70 60 50 bl; 40 'i: 30 20 10 11!:!INTERA Time concentration plots for MW-15 Sulfate in MW-15 Sample Date Uranium in MW-15 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values Time concentration plots for MW-17 Chloride in MW-17 40 30 20 0-1------r-------�---------�------------l �°'..,, �o Sample Date Fluoride in MW-17 0.8 -,------------------------------- 0.7 ·1----------------------------&.----l 0.6 ---------------------------&1�-----l 0.1 +--------------------------------1 0 -1-----,------.----�---.------.----�-----�-----I Sample Date l!IINTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values Time concentration plots for MW-17 Sulfate in MW-17 0 +---.......----.-----.------.---�---.----,-----.----1 1:°'"' �� 50 45 40 35 ::, 30 25 ·c 20 ::) 15 10 5 1:°'"' �� BINTERA Sample Date Uranium in MW-17 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values Time concentration plots for MW-18 Chloride in MW-18 0+-----.-----,---�--�--�---�--�---------l �"'"' �'1> 0.45 0.4 0.35 0.3 .§_ 0.25 -� 0.2 0.15 0.1 0.05 0 P, �o, �'1> �c::i"' �o l!IINTERA Sample Date Fluoride in MW-18 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values Time concentration plots for MW-18 Sulfate in MW-18 Sample Date Uranium in MW-18 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 Detected Values Non-Detected Values Time concentration plots for MW-19 Chloride in MW-19 100 90 80 70 :.-60 so 40 u 30 20 • 10 0 �°'"' �'Ii Sample Date Fluoride in MW-19 :.- 1t---��:---�•---1r11p1t-f�� .. -:-f�-...,,����� '; 0.8 ----------------------------------1"0 ·;: 0 :3 U:: 0.6 -1-----------------------------------1 �¼�NTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values ·2 Time concentration plots for MW-19 Sulfate in MW-19 0 +----.----,----..------.---�--�------�---I />"' �'Ii 20 15 10 Sample Date Uranium in MW-19 0-1---....--------�--�------�--�------1 �?>"' �'Ii Sample Date e Detected Values �¥s�NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •Non-Detected Values Time concentration plots for MW-20 Chloride in MW-20 80 ..------------------------------- 20 -1--------------------------------J 10 +------------------------------1 0+---....-----.---�--�------�--�------1 r:,'b �<:) �❖ � ...,.:s \'Ii ...,.:s BINTERA Sample Date Fluoride in MW-20 :<i◊ �i:� � � ,..� '(--'S �'Ii c.,•I� Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 i:� <:) e,? �", '(-q 0 �'Ii e Detected Values •Non-Detected Values 4500 4000 3500 3000 ] 2500 2000 1500 1000 500 0 (Jo,'• <;)q; (Jr:;. <;)q; 40 35 30 -25 20 ·2 15 10 5 0 (Jo,'" <;)q; i" <;)q; �¼�NTERA Time concentration plots for MW-20 Sulfate in MW-20 Sample Date Uranium in MW-20 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 • Detected Values Non-Detected Values 80 70 60 ::;-50 .§. GJ 40 ·;:: 30 20 10 0 r.;°>� "'q;r.:°>" "'q; 20 .§. QJ 15 ·;: 10 �¼�NTERA Time concentration plots for MW-22 Chloride in MW-22 Sample Date Fluoride in MW-22 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 • Detected Values Non-Detected Values 40 30 ·2 20 .--.-¥s�NTERA Time concentration plots for MW-22 Sulfate in MW-22 Sample Date Uranium in MW-22 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-23 Chloride in MW-23 35 �----------------------------� 30 ·t---------11---------------------------1 25 +------------------------------ 'iia 20 +--------------------------------1 Qj "C ·;: O 15 +---------11------------------------1 a l!IINTERA Sample Date Fluoride in MW-23 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values 90 80 70 60 i so ·2 40 30 20 10 5)'-> (\ ,xr:; .... ,>� �-i; BINTERA Time concentration plots for MW-23 r;:,°' �,,,.: Sulfate in MW-23 Sample Date Uranium in MW-23 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-24 Chloride in MW-24 80 70 60 _ 50 cu 40 30 20 10 0 c;;<, -Xe;; ...,.,j �'I> Sample Date Fluoride in MW-24 1.6 -,--------------------------------, 1.4 ------------------------------ 1.2 ------------------------------ 0 -----,-----,.---,-----,------.----.-----,-------,-----1 Sample Date �¾�NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values Time concentration plots for MW-24 Sulfate in MW-24 :'.j" 'oJi 2000 -1--------------......;;�---------------I .§. J!! .l!! :j 1500 -------------------------------1 250 200 :'.j" 150 ::I "i: l! ::, 100 50 0 I � l!!INTERA Sample Date Uranium in MW-24 --- Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 "- e Detected Values ■Non-Detected Values Time concentration plots for MW-24A Chloride in MW-24A 40 cu 30 ·;: 0 20 10 Sample Date Fluoride in MW-24A � 1.5 t-:.,;£C--------"t:,----------------------I cu "t:I ·;: 0 � 1+------------------------------------1 BINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values 10 9 8 7 ::. 6 'i: 4 ::::, 3 2 1 :f',i:."-.... � �� BINTERA Time concentration plots for MW-24A Sulfate in MW-24A Sample Date Uranium in MW-24A Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values 40 35 30 -25 20 15 10 5 0 !:)<, ..x.!:) ...,-s �,,, BINTERA Time concentration plots for MW-25 Chloride in MW-25 Sample Date Fluoride in MW-25 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values Time concentration plots for MW-25 Sulfate in MW-25 Sample Date Uranium in MW-25 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 Detected Values Non-Detected Values Time concentration plots for MW-26 Chloride in MW-26 100 90 80 70 = 60 50 ·;:: 0 40 u 30 20 10 s:i"' s:,l), � ,x�"' "" .,�q �<; '<vi 9,"" r;"> Q �'b �-s 0 Sample Date Fluoride in MW-26 � 0.6 +--+--+--------------------------1 � 0.5 0 i 0.4 ------¼----------�1-------------1--1-.U.---1 BINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 Detected Values ■Non-Detected Values Time concentration plots for MW-26 Sulfate in MW-26 :;-1500 ---------------------�--------- ] 1000 +------------------------------1 Sample Date Uranium in MW-26 } 80 +----------------___,. 'i: I.! 60 +----a--e---.hr-;HfHI- BINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values 0.9 � Time concentration plots for MW-27 Chloride in MW-27 Sample Date Fluoride in MW-27 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 Detected Values Non-Detected Values Time concentration plots for MW-27 Sulfate in MW-27 600 -.------------------------------ 200 +------------------------------1 100 +------------------------------1 0 ··1----�------�-----�--�---�--�---l !:)<, ">"� 35 30 25 Sample Date Uranium in MW-27 bQ 20 ·2 15 10 5 BINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values 180 160 140 120 r 100 80 60 40 20 0 !:>., � ff �'b.,_ ..,-s BINTERA Time concentration plots for MW-28 Chloride in MW-28 Sample Date Fluoride in MW-28 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 • Detected Values. Non-Detected Values � 'iia E Time concentration plots for MW-28 Sulfate in MW-28 3000 -r------------------------------� "; 1500 ·t-------------------------------1 J!! :i 1000 +------------------------------1 500 +------------------------------' 0 +-----,-------.---.----.....------r----.---.----�-----' Sample Date Uranium in MW-28 } 40 +--------------1..&--------------' ·2t! 30 +----------------1--------------------1 iii?,ri�NTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 :-,'b .,.,q •• Detected Values Non-Detected Values 45 40 35 30 } 25 ·;: 20 15 10 5 l:)<, � � �,,,-( '>" BINTERA Time concentration plots for MW-29 �o, �� Chloride in MW-29 Sample Date Fluoride in MW-29 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values Time concentration plots for MW-29 Sulfate in MW-29 � 2000 +-------------------------------1 .§. J!! .l!! :j 1500 +--------------'------------------! 60 50 40 30 ·2 20 ..... ... � 10 ,,,. j 0 l!!INTERA Sample Date Uranium in MW-29 ----..... -- Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 -Ao,._ ......... J � • ■ Detected Values Non-Detected Values �¾INTERA Time concentration plots for MW-30 Chloride in MW-30 Sample Date Fluoride in MW-30 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values Time concentration plots for MW-30 Sulfate in MW-30 800 600 400 Sample Date Uranium in MW-30 � 8+--,.,.-tt----Hi------tl� -� 6 �-----.;;.._--�1----+------------------l l!!INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values Time concentration plots for MW-31 Chloride in MW-31 450 400 350 300 '.:a 250 g 200 150 100 so 0 I:)<, � � �'I>� -.,..5 Sample Date Fluoride in MW-31 '.:a 0.8 f------➔+-----=��k----cAcft-.-----------,.._--11-:---ll---l g QJ "Cl ·;: g 0.6 +-------------------------------'---=----! BINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values Time concentration plots for MW-31 Sulfate in MW-31 1400 1200 1000 800 600 200 ·t-------------------------------1 0 +---.....-----,----.----...-------r-------r---.-----,-----l Sample Date Uranium in MW-31 Sample Date e Detected Values l!IINTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •Non-Detected Values 40 30 -� 20 �Sa�NTERA Time concentration plots for MW-32 Chloride in MW-32 Sample Date Fluoride in MW-32 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values Time concentration plots for MW-32 Sulfate in MW-32 Sample Date Uranium in MW-32 }4+--11-------------------------------� -� 3 +--ll-6---t--lft---------------------------1 �¼�NTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-35 Chloride in MW-35 0 +------r-----.---...------r-----.----.------r-----,--------l r.:"'� �e; Sample Date Fluoride in MW-35 b'.o 0.4 ._ __ ...,..... __ ___...,-------------11---i1-----�--------1 g 0.3 -1------------½,l'Ll�...,_---"lc,......--+--.,_---+--#--+>1---. l!!INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values :. '.a E Time concentration plots for MW-35 Sulfate in MW-35 3000 -.---------------------------------, "; 1500 ---------------------------------1.... � :i 1000 +-------------------------------1 500 +---------------------------------1 0 -·�--�--�------�---�--�--�-------! t:"'<::) Qe; 35 30 25 Sample Date Uranium in MW-35 '.a 20 E ·2 15 10 5 �¼�NTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •• Detected Values Non-Detected Values Time concentration plots for MW-36 Chloride in MW-36 Sample Date Fluoride in MW-36 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 Detected Values Non-Detected Values Time concentration plots for MW-36 Sulfate in MW-36 3500 �----------------------------� � 2000 +------------------------------1 .§. � .f! :i 1500 •1------------------------------l 1000 +------------------------------1 500 ------------------------------1 0 +---.....-------.-----,,----,-----,-----,-----,,----,-----1 Sample Date Uranium in MW-36 20 15 ·2 10 Sample Date e Detected Values �¥s�NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •Non-Detected Values 40 30 ·;;: 20 BINTERA Time concentration plots for MW-37 Chloride in MW-37 Sample Date Fluoride in MW-37 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values Time concentration plots for MW-37 Sulfate in MW-37 Sample Date Uranium in MW-37 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 Detected Values Non-Detected Values 50 45 40 35 :::i' 30 � 25 ·;: 20 15 · 10 5 0 ,i,:."'"b "b er.., �'Ii 0 �¼�NTERA Time concentration plots for MW-38 Chloride in MW-38 Sample Date Fluoride in MW-38 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values Time concentration plots for MW-38 Sulfate in MW-38 � 2000 _____________________________ _, :i 1500 -t-------------------------------1 Sample Date Uranium in MW-38 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 Detected Values Non-Detected Values 45 40 35 30 25 20 15 10 5 Time concentration plots for MW-39 Chloride in MW-39 Sample Date Fluoride in MW-39 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 Detected Values Non-Detected Values Time concentration plots for MW-39 Sulfate in MW-39 Sample Date Uranium in MW-39 _ 10 +---------------------------------1 E 8+---------------------------------1 ·1: � 6+---------------------------------1 •INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values •Non-Detected Values 0.9 0.8 0.7 0.6 E,. 0.5 ·;:: 0.4 0.3 0.2 0.1 0 'b ....... el �'I> 0 �¥-�NTERA Time concentration plots for MW-40 Chloride in MW-40 Sample Date Fluoride in MW-40 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values ■Non-Detected Values 20 15 'i: 10 BINTERA Time concentration plots for MW-40 Sulfate in MW-40 Sample Date Uranium in MW-40 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 e Detected Values ■Non-Detected Values Time concentration plots for TW4-24 Chloride in TW4-24 "iii; 800 -----...--��---------------..... --11---�-----1 GI :2 � 600 _________ _, __ ......,_...,... __________________ -1 Sample Date Fluoride in TW4-24 0.6 ..--------------------------------, 0.5 +------------------------------ 0+-----.------.-----,-----.------.----..-----,------,------1 Sample Date e Detected Values l!!INTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 •Non-Detected Values 800 600 ·c 400 BINTERA Time concentration plots for TW4-24 Sulfate in TW4-24 Sample Date Uranium in TW4-24 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2022 • Detected Values Non-Detected Values Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Goble, Kathy Weinel Monday, October 24, 2022 10:12 AM Phillip Goble 'Dean Henderson'; David Frydenlund; Scott Bakken; Garrin Palmer; Logan Shumway; Jordan Christine App Transmittal of CSV Files White Mesa Mill 2022 Q3 Groundwater Monitoring DTW All Programs Q3 2022.xlsx; Q3 2022 Analytical Data.csv; Q3 2022 GW Field Data.csv Attached to this e-mail is an electronic copy of laboratory results for groundwater monitoring conducted at the White Mesa Mill during the third quarter of 2022, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel ,CE Energy Fuels Resources (USA) Inc. Kathy Weinel Director, Regulatory Compliance t:303.389.4134 I c: I t:303.389.4125 KWeinel@energyfuels.com 225 Union Blvd., Suite 600 Lakewood, CO 80228 http://www.anerqyfuels.com This e-mail is intended for the exclusive use of person(s) mentioned as the recipient(s). This message and any attached files with it are confidential and may contain privileged or proprietary information. If you are not the intended recipient(s) please delete this message and notify the sender. You may not use, distribute print or copy this message if you are not the intended recipient(s). 1