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DRC-2022-020018 - 0901a068810cdd4e
August 8, 2022 Sent VIA OVERNIGHT DELIVERY Mr. Doug Hansen Director Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West Salt Lake City, UT 84116 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www. · nergyfuels.com Re: Transmittal of 2nd Quarter 2022 Groundwater Monitoring Report Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr. Hansen: Enclosed are two copies of the White Mesa Uranium Mill Groundwater Monitoring Report for the 2nd Quarter of 2022 as required by the Groundwater Quality Discharge Permit UGW370004, as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours very truly, (dtbf Jfr'it4 ENERGY FUELS RESOURCES (USA) INC. Kathy Weinel Director, Regulatory Compliance cc: David Frydenlund Scott Bakken Logan Shumway Garrin Palmer DRC-2022-020018 White Mesa Uranium Mill Groundwater Monitoring Report State of Utah Groundwater Discharge Permit No. UGW370004 2nd Quarter (April through June) 2022 Prepared by: eN:RGYFUELS Energy Fuels Resources (USA) Inc. 225 Union Boulevard, Suite 600 Lakewood, CO 80228 August 8, 2022 TABLE OF CONTENTS 1.0 INTRODUCTION ............................................................................................................... 1 2.0 GROUNDWATER MONITORING ................................................................................... 1 2.1 Samples and Measurements Taken During the Quarter.. ................................................. 1 2.1.1 Groundwater Compliance Monitoring ...................................................................... 1 2.1.2 Accelerated Groundwater Monitoring ...................................................................... 1 2.1.3 Background Well Monitoring ................................................................................... 2 2.1.4 TW4-24 ..................................................................................................................... 2 2.1.5 Parameters Analyzed ................................................................................................ 2 2.1.6 Groundwater Head Monitoring ................................................................................. 3 2.2 Field Data ......................................................................................................................... 3 2.3 Laboratory Results -Quarterly Sampling ........................................................................ 3 2.3.1 Copy of Laboratory Results ...................................................................................... 3 2.3 .2 Regulatory Framework and Groundwater Background ............................................ 4 2.4 Laboratory Results -Accelerated Monitoring ................................................................. 4 2.4.1 Copy of Laboratory Results ...................................................................................... 4 2.4.2 Regulatory Framework and Groundwater Background ............................................ 4 2.4.3 Compliance Status .................................................................................................... 5 2.5 Depth to Groundwater and Water Table Contour Map .................................................... 5 3.0 QUALITY ASSURANCE AND DATA VALIDATION ................................................... 5 3.1 Field QC Samples ............................................................................................................. 6 3.2 Adherence to Mill Sampling SOPs .................................................................................. 6 3.3 Analyte Completeness Review ......................................................................................... 7 3.4 Data Validation ................................................................................................................ 7 3.4.1 Field Data QNQC Evaluation .................................................................................. 7 3.4.2 Holding Time Evaluation .......................................................................................... 9 3.4.3 Receipt Temperature Evaluation ............................................................................... 9 3.4.4 Analytical Method Checklist .................................................................................... 9 3.4.5 Reporting Limit Evaluation ....................................................................................... 9 3.4.6 Trip Blank Evaluation ............................................................................................. 10 3.4.7 QNQC Evaluation for Routine Sample Duplicates ............................................... 10 3.4.8 Radiologies Counting Error and Duplicate Evaluation .......................................... 10 3.4.9 Other Laboratory QNQC ....................................................................................... 11 3.4.10 TDS Results ............................................................................................................ 14 4.0 CORRECTIVE ACTION REPORT .................................................................................. 14 4.1 5.0 6.0 7.0 Assessment of Corrective Actions from Previous Period .............................................. 14 TIME CONCENTRATION PLOTS .................................................................................. 14 ELECTRONIC DATA FILES AND FORMAT ............................................................... 14 SIGNATURE AND CERTIFICATION ............................................................................ 16 Table 1 Table 2 Table 3 LIST OF TABLES Summary of Well Sampling for the Period Exceedances and Acceleration Requirements GWCL Exceedances INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports -Quarterly Sampling Tab F Laboratory Analytical Reports -Accelerated Monitoring Tab G Quality Assurance and Data Validation Tables G-lA/B G-2A/B G-3A/B G-4AJB G-5AJB G-6AJB G-7A/B G-8A/B G-9AJB Field Data QA/QC Evaluation Holding Time Evaluation Laboratory Receipt Temperature Check Analytical Method Check Reporting Limit Evaluation Trip Blank Evaluation QA/QC Evaluation for Sample Duplicates Radiologies Counting Error Laboratory Matrix QC Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter ii coc CTF DWMRC EFRI GEL GWCLs GWDP LCS MS MSD QA QAP QC RPD SOPs USEPA Chain-of-Custody Chemtech-Ford ACRONYM LIST Utah Division of Waste Management and Radiation Control Energy Fuels Resources (USA) Inc. GEL Laboratories, Inc. Groundwater Compliance Limits Groundwater Discharge Permit Laboratory Control Spike Matrix Spike Matrix Spike Duplicate Quality Assurance Quality Assurance Plan Quality Control Relative Percent Difference Standard Operating Procedures United States Environmental Protection Agency 111 1.0 INTRODUCTION This is the Routine Groundwater Monitoring Report, as required under Part I.F.1 of State of Utah Groundwater Discharge Permit No. UGW370004 (the "GWDP") for the second quarter of 2022 for Energy Fuels Resources (USA) Inc.'s. ("EFRI's") White Mesa Uranium Mill (the "Mill"). As required under Parts I.E.1, 1.E.2, I.E.3, and I.E.5 of the GWDP, this Report includes recorded field measurements and laboratory analyses for well monitoring conducted during the quarter. 2.0 GROUNDWATER MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of groundwater monitoring wells, piezometers, existing wells, chloroform contaminant investigation wells and nitrate contaminant investigation wells is attached under Tab A. Groundwater samples and measurements were taken during this rep01ting period, as discussed in the remainder of this section. 2.1.1 Groundwater Compliance Monitoring Groundwater samples and field measurements collected during the quarter included quarterly, semi-annual and accelerated monitoring. Accelerated monitoring is discussed below in Section 2.1.2. In this report, samples classified as being collected quarterly include those wells which are routinely sampled every quarter and the wells sampled semi-annually. Wells which are sampled routinely every quarter and semi-annually were analyzed for the parameters listed in Table 2 and Part I.E.1.d) 2)ii of the GWDP. Table 1 of this report provides an overview of wells sampled during the current period, along with the required sampling frequency applicable to each well during the current monitoring period, the date samples were collected from each well, and the date(s) analytical data were received from the contract laboratory(ies). Table 1 also indicates which sample numbers are associated with the required duplicates. During this quarter, three wells were resampled. MW-26 was resampled for Gross Alpha minus radon and uranium ("gross alpha") and MW-27 and MW-32 were resampled for total dissolved solids ("TDS") because of laboratory issues. MW-26 was resampled for gross alpha on April 27, 2022 and MW-27 and MW-32 were resampled for TDS on May 16, 2022. 2.1.2 Accelerated Groundwater Monitoring Accelerated monthly sampling was also performed (quarterly wells accelerated to monthly), and results reported, for the wells indicated in Table 1. The accelerated sampling frequency, analyte list and well list were determined based on the previous analytical results as shown in Table 2. 1 Table 1 provides an overview of the wells sampled for the accelerated monthly program along with the routine sampling frequency as well as the accelerated sampling frequency, the date samples were collected from each well, the associated duplicates and the date(s) which analytical data were received from the contract laboratory(ies). 2.1.3 Background Well Monitoring Monitor wells MW-38, MW-39, and MW-40 were installed in the first quarter 2018 pursuant to the GWDP Part l.H.2 and quarterly sampling commenced in fourth quarter 2018. The GWDP Part 1.H.3 requires the completion of a background report for each of these wells after the completion of 8 quarters of sampling. The background reports and resultant Groundwater Compliance Limits ("GWCLs") were calculated based on eight statistically valid data points. The background report for wells MW-38, MW-39 and MW-40 was submitted to DWMRC on March 4, 2021. EFRI submitted errata pages by letter dated June 7, 2021 based on the DWMRC review comments. The Background Report for MW-38, MW-39 and MW-40 was approved by DWMRC by letter dated June 16, 2021. MW-38, MW-39 and MW-40 will continue to be sampled on a quarterly basis until such time as these wells are included in the GWDP. The analytical results for MW-38, MW-39, and MW-40 for this period are included in TabE. 2.1.4 TW4-24 Pursuant to the GWDP, Part l.E.l.c).ii, semi-annual monitoring of TW4-24 commenced in the second quarter of 2018. TW4-24 is currently used as a pumping well for the nitrate corrective action, is located within the chloroform plume, and is expected to exceed groundwater quality standards for analytes associated with these projects. It is expected that monitoring results will be highly variable as a result of the pumping and should not be used for direct compliance purposes. Rising or decreasing trends in analytes caused solely by pumping should not be unexpected. Further, as background cannot be established for this pumping well, and given the variability of background concentrations across the site, analyte concentrations in TW4-24 may also vary widely from site ranges due to natural background variability and/or localized changes resulting from long-term pumping. 2.1.5 Parameters Analyzed Routine quarterly groundwater monitoring samples were analyzed for the parameters listed in Table 2 and Part I.E. l.d) 2) ii of the GWDP. The accelerated monitoring samples were analyzed for a more limited and specific parameter list as shown in Table 2. 2 2.1.6 Groundwater Head Monitoring Depth to groundwater was measured in the following wells and/or piezometers, pursuant to Part I.E.3 of the GWDP: • The quarterly groundwater compliance monitoring wells (including MW-33 and MW-34). • Existing monitoring well MW-4 and the temporary chloroform investigation wells. • Piezometers -P-1, P-2, P-3A, P-4 and P-5. • Nitrate monitoring wells. • The DR piezometers which were installed during the Southwest Hydrogeologic Investigation. • In addition to the above, depth to water measurements are routinely observed m conjunction with sampling events for wells sampled during quarterly and accelerated efforts, regardless of the sampling purpose. Water levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab D. 2.2 Field Data Attached under Tab B are copies of field data sheets recorded in association with the quarterly effort for the groundwater compliance monitoring wells referred to in paragraph 2.1 .1, above. Sampling dates are listed in Table 1. Attached under Tab C are copies of the field data sheets recorded in association with the accelerated monthly monitoring sampling efforts, referred to in paragraph 2.1.2, above. Sampling dates are listed in Table 1. 2.3 Laboratory Results -Quarterly Sampling 2.3.1 Copy of Laboratory Results Analytical results are provided by two contract analytical laboratories: GEL and Chemtech-Ford ("CTF"). Table 1 lists the dates when analytical results were reported to the Director, Regulatory Compliance for each well. 3 Results from analysis of samples collected under the GWDP (i.e., regular quarterly and accelerated samples) are provided in Tab E. Also included under Tab E are the results of analyses for duplicate samples as identified in Table 1. 2.3.2 Regulatory Framework and Groundwater Background Under the GWDP, background groundwater quality has been determined on a well-by- well basis, as defined by the statistics contained in the Decision Tree/Flowchart used for the previous Background Reports that was conditionally approved by the DWMRC on August 24, 2007. GWCLs that reflect this background groundwater quality have been set for compliance monitoring wells. Exceedances of the GWCLs during the preceding quarter determined the accelerated monthly monitoring program implemented during this quarter as noted in Tables 1 and 2. Exceedances of the GWCLs for this quarter are listed in Table 2 for sampling required under the revised GWDP. Accelerated requirements resulting from this quarter are highlighted for ease of reference. Table 3 documents the accelerated sampling program and shows the results and frequency of the accelerated sampling conducted. It should be noted, however, that, because the GWCLs have been set at the mean plus second standard deviation, or the equivalent, un-impacted groundwater would normally be expected to exceed the GWCLs approximately 2.5% of the time. Therefore, exceedances are expected in approximately 2.5% of sample results, and do not necessarily represent impacts to groundwater from Mill operations. In fact, more frequent sampling of a given analyte will increase the number of exceedances due to statistical variation and not due to Mill activity. Additionally, given the slow velocity of groundwater movement, accelerated sampling monthly may result in resampling of the same water and may lead to repeat exceedances for accelerated constituents not due to Mill activities, but due to repeat sampling of the same water. 2.4 Laboratory Results -Accelerated Monitoring 2.4.1 Copy of Laboratory Results Results from analysis of samples collected for the monthly accelerated sampling (i.e. quarterly accelerated to monthly) are provided in Tab F. Also included under Tab Fare the results of analyses for duplicate samples for this sampling effort, as identified in Table 1. 2.4.2 Regulatory Framework and Groundwater Background As a result of the issuance of a revised GWDP on March 8, 2021, which sets revised GWCLs, requirements to perform accelerated monitoring under Part I.G. l of the previous GWDP ceased, effective March 8, 2021, and the effect of the issuance of the revised GWDP was to create a "clean slate" for most constituents going forward. 4 This means that accelerated monitoring during this quarter was required under the revised GWDP for only those constituents that exceeded the GWCLs since March 8, 2021. 2.4.3 Compliance Status Analytes that have exceeded the GWCLs set forth in the GWDP are summarized in Table 2. The analytes which exceeded their respective GWCLs during the quarter will be sampled on an accelerated schedule as noted in Table 2. A review of the accelerated data collected during the quarter is reported in EFRI's Exceedance Notice for the quarter. Part I.G.4 c) of the GWDP states, with respect to exceedances of GWCLs, "The Permittee shall prepare and submit within 30 calendar days to the Executive Secretary a plan and a time schedule for assessment of the sources, extent and potential dispersion of the contamination, and an evaluation of potential remedial action to restore and maintain groundwater quality to insure that Permit limits will not be exceeded at the compliance monitoring point and that DMT or BAT will be reestablished." EFRI submits an Exceedance Notice quarterly and the summary in the Exceedance Notice includes, for each exceedance, a brief discussion of whether such a plan and schedule is required at this time in light of other actions currently being undertaken by EFRI. The determination of whether a Plan and Time Schedule is required is based on discussions with DWMRC Staff in teleconferences on April 27 and May 2, 2011 and the constituents covered by previously submitted Source Assessment Reports. 2.5 Depth to Groundwater and Water Table Contour Map As stated above, a listing of groundwater level readings for the quarter (shown as depth to groundwater in feet) is included under Tab D. The data from Tab D has been interpreted (kriged) and plotted in a water table contour map, provided under Tab H. The water table contour map provides the location and identity of the wells and piezometers for which depth to groundwater is recorded. The groundwater elevation at each well and piezometer, measured in feet above mean sea level, and isocontour lines to delineate groundwater flow directions observed during the quarter's sampling event are displayed on the map. 3.0 QUALITY ASSURANCE AND DATA VALIDATION The Mill Director, Regulatory Compliance performed a Quality Assurance/Quality Control ("QA/QC") review to confirm compliance of the monitoring program with requirements of the Groundwater Monitoring Quality Assurance Plan ("QAP"). As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and quality control review of laboratory data methods and data. Identification of field QC samples collected and analyzed is provided in Section 3.1. Discussion of adherence to Mill sampling Standard Operating Procedures ("SOPs") is provided in Section 3.2. Analytical 5 completeness review results are provided in Section 3.3. The steps and tests applied to check laboratory data QA/QC are discussed in Sections 3.4.4 through 3.4.9 below. The Analytical Laboratories have provided summary reports of the analytical QA/QC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference certification and reporting protocol. The analytical laboratory QA/QC Summary Reports, including copies of the Mill's COC and Analytical Request Record forms for each set of Analytical Results, follow the analytical results under Tabs E and F. Review of the laboratory QA/QC information is provided under Tab G. 3.1 Field QC Samples The following field QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program: Two duplicate samples were collected during quarterly sampling as indicated in Table 1. The QC samples were sent blind to the analytical laboratory and analyzed for the same parameters as permit-required samples. One duplicate sample was collected during each month of accelerated sampling as indicated in Table 1. The QC samples were sent blind to the analytical laboratory and analyzed for the same accelerated parameters as the parent sample. Four trip blanks were provided by CTF and returned and analyzed with the quarterly monitoring samples. One trip blank for each of the monthly accelerated sample events was provided by CTF and returned and analyzed with the accelerated monthly monitoring samples. Rinsate samples were not collected during the quarter because equipment used during sample collection was dedicated and did not require decontamination. All wells except MW-20, MW-24, MW-37 and MW-38 have dedicated pumps for purging and sampling and as such no rinsate blanks samples are required. MW-20, MW-24, MW-37 and MW- 38 were purged and sampled with a disposable bailer and no rinsate blank was required. A deionized field blank was not required because equipment decontamination was not required and deionized water was not used during this sampling event. 3.2 Adherence to Mill Sampling SOPs On a review of adherence by Mill personnel to the existing sampling SOPs, the Director, Regulatory Compliance observed that QA/QC requirements established in the QAP were met and that the SOP's were implemented as required. 6 3.3 Analyte Completeness Review Analyses required by the GWDP for the quarterly and accelerated wells were performed. The accelerated sampling for the quarterly wells (quarterly to monthly) was completed as required by the GWDP and as shown in Tables 2 and 3. The monthly accelerated sampling program shown on Tables 2 and 3 is required as a result of exceedances in quarterly well monitoring results reported in previous quarters. 3.4 Data Validation The QAP and GWDP identify the data validation steps and data quality control checks required for the groundwater monitoring program. Consistent with these requirements, the Director, Regulatory Compliance completed the following evaluations: a field data QNQC evaluation, a receipt temperature check, a holding time check, an analytical method check, a reporting limit check, a trip blank check, a QNQC evaluation of routine sample duplicates, a QA/QC evaluation of accelerated sample duplicates, a gross alpha counting error evaluation and a review of each laboratory's reported QNQC information. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab G. 3.4.1 Field Data QA/QC Evaluation The Director, Regulatory Compliance performs a review of field recorded parameters to assess their adherence with QAP requirements. The assessment involved review of two sources of information: the Field Data Sheets and the Quaiterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and the stability of the following field parameters (based upon the purging method chosen): specific conductance, pH, temperature, redox potential, dissolved oxygen ["DO"] and turbidity. Stability of field parameters and well sampling techniques are dependent on the purging technique employed. Review of the Depth to Water data confirms that depth measurements were conducted within a five-day period. The results of this quarter's review are provided in Tab G. There are three purging strategies specified in the QAP that are used to remove stagnant water from the casing during groundwater sampling at the Mill. The three strategies are as follows: 1. Purging three well casing volumes with a single measurement of field parameters 2. Purging two casing volumes with stable field parameters (within 10% [Relative Percent Difference] ("RPD")) 3. Purging a well to dryness and stability (within 10% RPD) of a limited list of field parameters after recovery During both the quarterly sampling event and the two monthly events, the purging technique used was two casing volumes with stable field parameters (pH, Conductivity, 7 Redox, temperature, DO, and turbidity) except for the following wells that were purged to dryness after 2 casing volumes were removed: MW-03A, MW-23, MW-24, and MW- 24A. Based upon the review of the Field Data Sheets, quarterly and semi-annually sampled locations conformed to the QAP requirement for purging using the two casing volume technique except for MW-20, MW-37 and MW-38. MW-20, MW-37 and MW-38 were evacuated to dryness before two casing volumes could be removed. MW-20, MW-37 and MW-38 have insufficient water to purge using a pump. Due to the small volume of water present, these wells are purged and sampled using a disposable bailer. MW-20, MW-37 and MW-38 conformed to the QAP, requirement for sampling low yield wells which includes the collection of three field parameters (pH, specific conductance ["conductivity"] and temperature) immediately prior to and immediately following sample collection. Stabilization of pH, conductivity and temperature were within the 10% RPD required by QAP. MW-03A, MW-23, MW-24, and MW-24A were purged to dryness after 2 casing volumes were removed and the low yield sampling procedures were used for the collection of field parameters. Stabilization of pH, conductivity and temperature were within the 10% RPO required by QAP for well MW-03A, MW-23, MW-24 and MW-24A. Additionally, two casing volumes were not purged from MW-26 and TW4-24, prior to sampling because MW-26 and TW4-24 are continuously pumped wells. If a well is continuously pumped, it is pumped on a set schedule per the remediation plan and is considered sufficiently evacuated to immediately collect a sample; however, if a pumping well has been out of service for 48 hours or more, EFRI follows the purging requirements outlined in Attachment 2-3 of the QAP. The review of the field sheets for compliance with QAP requirements resulted in the observations noted below. The QAP requirements in Attachment 2-3 specifically state that field parameters must be stabilized to within 10% over at least two consecutive measurements. The QAP Attachment 2-3 states that turbidity should be less than 5 NTU prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP Attachment 2-3 does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements greater than 5 NTU below are included for information purposes only. • Turbidity measurements were less than 5 NTU for the quarterly and semi-annual wells except MW-11, MW-22, MW-29, MW-32, and MW-32 Resample. Per the QAP, Attachment 2-3, turbidity measurements prior to sampling were within a 10% RPD for the quarterly and semi-annual wells. • Turbidity measurements were less than 5 NTU for the accelerated sampling wells except MW-25 and MW-31 in the May monthly event and MW-11 in the June monthly event. As previously noted, the QAP does not require that turbidity be less than 5 NTU. Turbidity measurements prior to sampling were within a 10% RPD for the accelerated sampling wells 8 The other field parameters ( conductance, pH, redox potential, DO and temperature) for the wells were within the required RPD for the quarterly, semi-annual and accelerated sampling. During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water for the quarterly, semi-annual and accelerated sampling programs to the nearest 0.01 foot. EFRI's letter to DWMRC of March 26, 2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In response to DWMRC's subsequent correspondence dated June 1, 2010 and June 24, 2010, EFRI has completed a monitoring well redevelopment program. The redevelopment report was submitted to DWMRC on September 30, 2011. DWMRC responded to the redevelopment report via letter on November 15, 2012. Per the DWMRC letter dated November 15, 2012, the field data generated this quarter is compliant with the turbidity requirements of the approved QAP. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided under Tab G. The samples were received and analyzed within the required holding time. 3.4.3 Receipt Temperature Evaluation COC sheets were reviewed to confirm compliance with the QAP requirement in Table 1 that samples be received at 6°C or lower. Sample receipt temperature checks are provided under Tab G. The quarterly, semi-annual and accelerated samples were received within the required temperature limit. As noted in Tab G, samples for gross alpha analyses were shipped without using ice. Per Table 1 in the approved QAP, samples submitted for gross alpha analyses do not have a sample temperature requirement. 3.4.4 Analytical Method Checklist The analytical methods reported by both laboratories were checked against the required methods specified in the QAP. Analytical method check results are provided in Tab G. The review indicated that the quarterly, semi-annual and accelerated samples were analyzed in accordance with Table 1 of the QAP. 3.4.5 Reporting Limit Evaluation The analytical method RLs reported by both laboratories were checked against the RLs specified in the QAP Table 1. RL evaluations are provided in Tab G. The analytes were 9 measured and reported to the required RLs except that several sets of quarterly, semi- annual and accelerated sample results had the RL raised for at least one analyte due to matrix interference and/or sample dilution as noted in Section 3.4.9. In all cases the reported value for the analyte was higher than the increased RL. 3.4.6 Trip Blank Evaluation The trip blank results were reviewed to identify any VOC sample contamination which is the result of sample handling and shipment. Trip blank evaluations are provided in Tab G. The trip blank results associated with the quarterly, semi-annual and accelerated samples were all nondetect for VOCs. 3.4.7 QA/QC Evaluation for Routine Sample Duplicates Section 9 .1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results are less than 5 times the detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for the duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits; however, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPD is greater than 20%. The additional duplicate information is provided for information purposes. Field duplicate sample results were assessed as required by the SOP. Duplicate results were within the acceptance limits specified in the QAP except for ammonia and fluoride in MW-29/MW-65 and nitrate in MW-36/MW-70. The ammonia, fluoride and nitrate results were greater than 20% RPO, however, the sample and duplicate results were not greater than 5 times the RL and as such are acceptable. Field duplicate results are shown in Attachment G. The duplicate results were within a 20% RPD m the monthly accelerated samples. Results of the RPD test are provided under Tab G. 3.4.8 Radiologies Counting Error and Duplicate Evaluation Section 9 .14 of the QAP requires that when gross alpha results are reported with an activity equal to or greater than the GWCL the counting variance shall be equal to or less than 20% of the reported activity concentration. An error term may be greater than 20% of the repmted activity concentration when the sum of the activity concentration and error term is less than or equal to the GWCL. The quarterly and semi-annual radiologic sample results met the counting error requirements specified in the QAP except as noted in Tab G. The results for MW-22, MW-27, MW-32, and MW-39 did not meet the requirement that the counting error be equal to or less than 20% of the reported activity 10 concentration, likely because the reported concentrations are very near the RL. As stated above the error term may be greater than 20% of the reported activity concentration when the sum of the activity concentration and error term is less than or equal to the GWCL; however, MW-22 and MW-39 do not have a GWCL and this second level check cannot be performed. MW-27 and MW-32 passed the secondary check. The results are usable for the intended purpose and there is no adverse effect on the data. Section 9.4 of the QAP also requires a comparability check between the sample and field duplicate sample results utilizing the formula provided in the text. All of the radiologic duplicates were within acceptance limits or were nondetect. All of the radiologic duplicates were within acceptance limits. Results of quarterly, semi- annual, and accelerated radiologic sample QC are provided under Tab G. 3.4.9 Other Laboratory QA/QC Section 9.2 of the QAP requires that the laboratory's QA/QC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate analytical laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limit , (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, EFRI's Director, Regulatory Compliance rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-pecific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided under Tab G. The lab QA/QC results from both GEL and AW AL samples for compounds regulated under the GWDP met these requirements. The check samples included at least the following: a method blank, a laboratory control spike ("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the equivalent, where applicable. It should be noted that: • Laboratory fortified blanks are equivalent to LCSs. • Laboratory reagent blanks are equivalent to method blanks. • Post digestion spikes are equivalent to MSs. • Post digestion spike duplicates are equivalent to MSDs. • Laboratory Duplicates are equivalent to MSDs. The qualifiers, and the corresponding explanations reported in the QA/QC Summary Reports for the check samples for the analytical methods were reviewed by the Director, Regulatory Compliance. 11 The QAP, Section 8.1.2 states that an MS/MSD pair may be analyzed with each analytical batch depending on the analytical method specifications. The QAP does not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the MS/MSD pair be prepared on EFRI samples only. Acceptance limits for MS/MSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the specifications in the analytical methods to analyze either an MS or MS/MSD pair with each analytical batch were met as applicable to each method. While the QAP does not require it, the recoveries were reviewed for compliance with the laboratory established acceptance limits. The QAP does not require this level of review and the results of this review are provided for information only. The information from the Laboratory QA/QC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for the quarterly and semi-annual samples were within acceptable laboratory limits for the regulated compounds except as indicated in Tab G. The data recoveries and RPDs which are outside the laboratory established acceptance limits do not affect the quality or usability of the data because the recoveries and RPDs above or below the acceptance limits are indicative of matrix interference most likely caused by other constituents in the samples. Matrix interferences are applicable to the individual sample results only. The specifications in the analytical methods to analyze a MS/MSD pair with each analytical batch (as applicable to the methods) was met and as such the data are compliant with the QAP. The information from the Laboratory QA/QC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for the accelerated samples were within acceptable laboratory limits for the regulated compounds except as indicated in Tab G. The data recoveries and RPDs which are outside the laboratory established acceptance limits do not affect the quality or usability of the data because the recoveries and RPDs above or below the acceptance limits are indicative of matrix interference most likely caused by other constituents in the samples. Matrix interferences are applicable to the individual sample results only. The specifications in the analytical methods to analyze a MS/MSD pair with each analytical batch (as applicable to the methods) was met and as such the data are compliant with the QAP. The QAP specifies that surrogate compounds shall be employed for all organic analyses but the QAP does not specify acceptance limits for surrogate recoveries. The information from the Laboratory QA/QC Summary Reports indicates that the surrogate recoveries for the quarterly and accelerated samples were within acceptable laboratory limits for the surrogate compounds. The information from the Laboratory QA/QC Summary Reports indicates that the LCS recoveries for both the quarterly and accelerated samples were within acceptable laboratory limits except for iron, acetone and tetrahydrofuran in the quarterly samples and methyl ethyl ketone (2-butanone or MEK) in the accelerated monthly samples. Tetrahydrofuran, MEK and iron had high recoveries which is indicative of a high bias to the sample results. A high bias results in a more conservative data application. EFRI does not believe the data quality has been affected. 12 The low acetone LCS recovery is indicative of a low bias to the sample results. The data were flagged in accordance with the changes specified in EPA Method 8260D. The flagging requirements are new to the revised method and do not adversely affect the data. The data are usable for the intended purpose because there are no recent or historical detections of acetone in any onsite wells and the nondetect data are likely accurate. The QAP, Section 8.1.2 requires that each analytical batch shall be accompanied by a method blank. The analytical batches routinely contain a blank, which is a blank sample made and carried through all analytical steps. For the Mill samples, a method blank was prepared for the analytical methods. Per the approved QAP, contamination detected in analysis of method blanks will be used to evaluate any analytical laboratory contamination of environmental samples. The QAP states that non-conformance conditions will exist when contaminant levels in the samples(s) are not an order of magnitude greater than the blank result. All method blanks for both the quarterly and accelerated samples were nondetect. Method blank results are included in Tab E and Tab F. Laboratory duplicates are completed by the analytical laboratories as required by the analytical method specifications. Acceptance limits for laboratory duplicates are set by the laboratories. The QAP does not require the completion of laboratory duplicates or the completion of a QA assessment of them. EFRI reviews the QC data provided by the laboratories for completeness and to assess the overall quality of the data provided. Duplicate results for the quarterly, semi-annual and accelerated samples outside of the laboratory established acceptance limits are included in Tab G. The results outside of the laboratory established acceptance limits do not affect the quality or usability of the data because the RPDs above the acceptance limits are indicative of non-homogeneity in the sample matrix. Matrix affects are applicable to the individual sample results only. During the review, it was noted that recovery for one laboratory duplicate for TDS could not be completed due to the high concentrations present in the sample. The data are usable for the intended purpose because the results are indicative of a non-homogeneity in the sample matrix. The information from the Laboratory QA/QC Summary Reports indicates that there were low Continuing Calibration Verification ("CCV") recoveries for carbon tetrachloride, chloroform and chloromethane. The low CCV recoveries affected samples as follows: • MW-1, MW-2, MW-18, MW-19, MW-25, MW-27, MW-29, MW-31, MW-32, MW-35, MW -65 and trip blank; ( carbon tetrachloride, chloroform and chloromethane ); and • MW-20, MW-37 and trip blank (chloromethane). The data were flagged in accordance with the changes specified in EPA Method 8260D. The flagging requirements are new to the revised method and do not adversely affect the data. The data are usable for the intended purpose because carbon tetrachloride, 13 chloroform and chloromethane in the wells listed above do not have recent historical detections of carbon tetrachloride, chloroform and chloromethane and the nondetect data are likely accurate. 3.4.10 TDS Results The TDS results for several samples in analytical batch 22D 1197 were noted by the laboratory as inaccurate and biased high due to a laboratory error. The samples noted as having a high biased TDS results are: MW-31, MW-02, MW-25, MW-35, MW-18, and MW-19. EFRI was notified of this issue in May, well over a month after some of the samples had been collected. Upon review of the data EFRI resampled MW-27 and MW- 32, because the reported results for those samples were excessively high when compared to historic values. The remainder of the samples were not resampled due to time constraints and because the results were biased high, but not excessively so. The biased high results are reported herein and are used for compliance purposes, because reanalysis was not possible due to expired holding times. A high bias results in a more conservative data application. The laboratory did reanalyze the samples beyond the method allowable holding time and the reanalysis results were more consistent with historical results. The reanalysis data package is included in Tab E, behind the blue divider sheet, for information purposes only. The out of hold time data are not used for reporting or compliance. EFRI is working with CTF to prevent this issue from recurring. CTF has retrained all analysts and is monitoring the situation. 4.0 CORRECTIVE ACTION REPORT There are no corrective actions required during the current monitoring period. 4.1 Assessment of Corrective Actions from Previous Period No corrective actions were identified in the previous report. 5.0 TIME CONCENTRATION PLOTS Time concentration plots for each monitoring well for the following constituents: chloride, fluoride, sulfate, and uranium, are included under Tab I. The data points collected to date are reflected on the plots. Time concentration plots included with quarterly groundwater reports prior to and including first quarter 2012 did not include data that were determined to be outliers using the statistical methods used for the background determinations at the Mill. Based on conversations with DWMRC, all of the data have been included in the quarterly time concentration plots since first quarter 2012. 6.0 ELECTRONIC DATA FILES AND FORMAT 14 EFRI has provided to the Director electronic copies of the laboratory results from groundwater quality monitoring conducted during the quarter in Comma Separated Values format, from the analytical laboratories. A copy of the transmittal e-mail is included under Tab J. 15 7.0 SIGNATURE AND CERTIFICATION This document was prepared by Energy Fuels Resources (USA) Inc. Energy Fuels Resources (USA) Inc. By: t\~\~2 Scott A. Bakken Date Vice President, Regulatory Affairs 16 Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Scott A. Bakken Vice President, Regulatory Affairs Energy Fuels Resources (USA) Inc. 17 INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab C 1 Field Data Worksheets Accelerated Monitoring, May 2022 Tab C2 Field Data Worksheets Accelerated Monitoring, June 2022 Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports -Quarterly Sampling Tab F Laboratory Analytical Reports -Accelerated Monitoring Tab Fl Laboratory Analytical Reports -Accelerated Monitoring, May 2022 Tab F2 Laboratory Analytical Reports -Accelerated Monitoring, June 2022 Tab G Quality Assurance and Data Validation Tables G-lA/B G-2A/B G-3A/B G-4AIB G-5AIB G-6AIB G-7A/B G-8 A/B G-9AIB Field Data QA/QC Evaluation Holding Time Evaluation Laboratory Temperature Check Analytical Method Check Reporting Limit Evaluation Trip Blank Evaluation QA/QC Evaluation for Sample Duplicates Radiologies Counting Error Laboratory Matrix QC Tab H Kriged Current Quarterly Groundwater Contour Map Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter Tables Table I: Summary of Well Sampling for the Quarter Normal Purpose for sampling this Well Frequency quarter Sample Date Date of Lab Report MW-01 Semi-annually General Monitoring Well 04/14/22 (5/26/22 6/2122) [5/16/22] MW-02 Semi-annually Semi-annually 04/12/22 (5/26/22 6/2122) [5/16/22] MW-03A Semi-annually Semi-annually 04/27/22 (6/2/22) [5/26/22 6/1/22] MW-05 Semi-annually Semi-annually 04/18/22 (6/2/22) (5/23/22] MW-11 Quarterly Quarterly 04/18/22 (6/2/22) (5/23/22] MW-12 Semi-annually Semi-annually 04/19/22 (6/2/22) (5/23/22] MW-14 Quarterly Quarterly 04/18/22 (6/2/22) [5/23/22] MW-15 Semi-annually Semi-annually 04/19/22 (6/2/22) (5/23/22] MW-17 Semi-annually Semi-annually 04/18/22 ( 6/2/22) [ 5/23/22] MW-18 Semi-annually General Monitoring Well 04/13/22 (5/26/22 6/2/22) [5/16/22] MW-19 Semi-annually General Monitoring Well 04/13/22 (5/26/22 6/2/22) [5/16/22] MW-20 Semi-annually General Monitoring Well 05/17/22 (6/3/22 6/3122) (6/16/22] MW-22 Semi-annually General Monitoring Well 04/25/22 (6/2/22) [5/26/22 6/1/22] MW-23 Semi-annually Semi-annually 04/27/22 (6/2/22) [5/26/22 611/22] MW-24 Semi-annually Semi-annually 04/27/22 (6/2/22) [5/26/22 611/22] MW-24A Semi-annually Semi-annually 04/27/22 (6/2/22) [5/26/22 6/1/22] MW-25 Quarterly Quarterly 04/12/22 (5/26/22 612/22) [5/16/22] MW-26 Quarterly Quarterly 04/20/22 (6/2/22) MW-26 Resample Quarterly Quarterly 04/27/22 [5/26/22 6/1122] MW-27 Semi-annually Semi-annually 04/12/22 (5/26/22 6/2/22) (5/16/22] MW-27 Resample Semi-annually Semi-annually 05/16/22 (6/3/22 6/3/22) MW-28 Semi-annually Semi-annually 04/19/22 (6/2/22) (5/23/22] MW-29 Semi-annually Semi-annually 04/14/22 (5/26/22 612122) [5/16/22] MW-30 Quarterly Quarterly 04/20/22 (6/2/22) (5/23/22] MW-31 Quarterly Quarterly 04/11/22 (5/26/22 612/22) [5/16/22] MW-32 Semi-annually Semi-annually 04/11/22 (5/26/22 6/2/22) [5/16/22] MW-32 Resample Semi-annually Semi-annually 05/16/22 (6/3/22 6/3122) MW-35 Semi-annually Semi-annually 04/12/22 (5/26/22 6/2/22) [5/16/22] MW-36 Quarterly Quarterly 04/21/22 (6/2/22) (5/23/22] MW-37 Semi-annually Semi-annually 05/17/22 (6/3/22 6/3122) [6/16/22] MW-38 Background Background 04/27/22 (6/2/22) [5/26/22 6/1122] MW-39 Background Background 04/20/22 (6/2/22) (5/23/22] MW-40 Background Background 04/19/22 (6/2/22) [5/23/22] TW4-24 Semi-annually General Monitoring Well 04/27/22 (6/2/22) (5/26/22 6/1/22] MW-65 1 per Batch Duplicate of MW-29 04/14/22 (5/26/22 612/22) [5/16/22] MW-70 1 per Batch Du pllcatc of MW -3 6 04/21/22 (612m) (512:11221 Accelerated May Monthly MW-11 Monthly Accelerated 05/04/22 (6/3/22 7112/22 ) MW-25 Monthly Accelerated 05/03/22 (6/3/22 7112/22) MW-26 Monthly Accelerated 05/04/22 (6/3/22 7/12122) MW-30 Monthly Accelerated 05/04/22 (6/3/22 7112122) MW-31 Monthly Accelerated 05/03/22 ( 6/3/22 7 I I 2/22 ) MW-65 1 per Batch Duplicate of MW-30 05/04/22 (6/3/22 7112/22) Accelerated June Monthly MW-11 Monthly Accelerated 06/06/22 (6/22/22) MW-25 Monthly Accelerated 06/07/22 (6/22/22) MW-26 Monthly Accelerated 06/07/22 (6/22/22) MW-30 Monthly Accelerated 06/07/22 (6/22/22) MW-31 Monthly Accelerated 06/06/22 (6/22/22) MW-65 1 per Batch Duplicate of MW-25 06/07/22 (6/22/22) No1c : Muiliple dates shown for a single laboratory depict resubmission dates for the data. Resubmissions were required to correct reporting errors. When mulliple dates are shown for a single laboratory, the final submission date is shown in ilalics. Dates in parenthesis depicts the date that data was reported by Chemtech-Ford (CTF). Dates in brackets are the date and data reported by GEL Laboratories. Table 2 Exceedances and Acceleration Rcquircmcnls Monitoring Well GWCLin First Result Routine Sample Accelerated Exceedance Start of Accelerated (Water Class) Constituent Exceeding GWCL Current Exceeding the Frequency Frequency Sample Period Monitoring GWDP GWCL Q1mrterly Wells Accelerated to Monthly Sampling MW-I I (Class II) Total Dissolved Solids (mg/L) 2528 2680 Quarterly Monthly Q3 2021 November 2021 Manganese (ug/L) 237 376 Quarterly Monthly Q3 2021 November 2021 Nitrate + Nitrite (as N) (mg/L) 2.5 2.55 Quarterly Monthly QI 2022 June 2022 Chloride (mg/L) 39.16 48.4 Quarterly Monthly Q3 2019 Q4 2019 (November) Sulfate {mg/L) 1309 1410 Quarterly Monthly Q3 2019 Q4 2019 (November) MW-25 (Class III) Total Dissolved Solids (mg/L) 2976 3100 Quarterly Monthly Q3 2021 November 2021 MW-26 (Class Ill) Nitrate+ Nitrite (as N) (mg/L) 0.62 1.3 Quarterly Monthly QI 2010 May 2010 Chloroform (ug/L) 70 700 Quarterly Monthly QI 2010 May 2010 Total Dissolved Solids (mg/L) 3284. I 9 3390 Qum1erly Monthly Q3 2021 November 2021 Chloride (mg/L) 58.31 72 Quarterly Monthly QI 2010 May2010 Carbon Tetrachloride (ug/L) 5 26.1 Qum1erly Monthly Ql 2021 Q2 2021 Methylene Chloride (ug/L) 5 6.59 Quarterly Monthly Q3 2020 August 2020 MW-30 (Class II) Nitrate+ Nitrite (as N) (mg/L) 2.5 16.1 Quarterly Monthly Ql 2010 May 2010 Chloride (mg/L) 128 134 Quarterly Monthly Ql 2011 May201 I Total Dissolved Solids (mg/L) 1918 2010 Quarterly Monthly Q3 2021 November 2021 Selenium (ug/L) 53.6 56.3 Qua11erly Monthly Ql 2021 Q22021 Uranium (ug/L) 9.82 10.2 Quarterly Monthly QI 2021 Q2 2021 MW-3 1 (Class III) Nitrate+ Nitrite (as N) (mwL) 5 21.7 Quarterly Monthly Ql 2010 May 2010 Total Dissolved Solids (mg/L) 2132 2580 Quunorly Momhly Q3 2019 Q4 2019 (November) Uranium (ug/L) 15 15.5 Quarterly Monthly Q2 2020 August 2020 Sulfate (mg/L) 993 1150 Quanerl)• Monthly QJ 2019 Q4 2019 (November) Chloride (mg/L) 143 145 Quurtcrly Momhly QI 2011 Mny2011 Semi-Annual Wells Accelerated to Quarterly Sompling Monitoring Well GWCLin First Result Sample Accelerated Exceedance Start of Accelerated Constituent Exceeding GWCL Current Exceeding the (Water Class) GWDP GWCL Frequency Frequency Sample Period Monitoring MW-12 (Class Ill) Uranium (ug/L) 23.5 23.7 Semi-Annually Quarterly Q2 2017 Q3 2017 Selenium (ug/L) 39 41.2 Semi-Annually Quarterly Q2 2020 Q3 2020 MW-24 (Class III) Cadmium (ug/L) 6.43 6.97 Semi-Annually Quarterly Q2 2018 Q3 2018 (September) Beryllium (ug/L) 2 2.42 Semi-Annually Quarterly Q4 2017 QI 2018 Thallium (ug/L) 2.01 2.44 Semi-Annually Quarterly Q2 2018 Q3 2018 (September) Nickel (ug/L) 50 57.7 Semi-Annually Quarterly Q4 2018 Q3 2019 Sulfate (mg/L) 2903 2960 Semi-Annually Quarterly QI 2020 Q3 2020 Mnn~anese (ug/L) 7507 7700 Semi-Annually Quarterly Q4 2019 QI 2020 Fluoride (mg/L) 0.47 0.797 Semi-Annually Quarterly Q4 2018 Q3 2019 Gross Alpha (pCi/L) 7.5 9.03 Semi-Annually Quarterly Q4 2020 Q3 2021 TDS (mg/L) 4450 4460 Semi-Annually Quarterly Q2 2021 Q3 2021 Field pH (S.U.) 5.03 4.45 Semi-Annually Quarterly Q2 2018 03 2018 (September) MW-27 (Class III) Nitrate+ Nitrite (as N) (mg/L) 5.6 5.8 Semi-Annually Quarterly Q2 2010 Q3 2010 Fluoride (mg/LJ 0.85 0.90 Semi-Annually Quarterly Q2 2022 Q3 2022 MW-28 (Class lll) Chloride (mg/L) 105 108 Semi-Annually Quarterly Q2 2010 Q3 2010 Nitrate+ Nitrite (as N) (mg/L) 5 5.14 Semi-Annually Quarterly Q4 2019 Q3 2020 Selenium (ug/L) 11. I 12.4 Semi-Annually Quarterly Q2 2019 Q3 2019 Cadmium (ug/L) 5.2 5.41 Semi-Annually Quarterly Q2 2014 Q4 2014 Uranium (ug/L) 4.9 61.3 Semi-Annually Quarterly Q2 2014 Q4 2014 MW-29 (Class III) Uranium (ug/L) 15 15.3 Semi-Annually Quarterly Q42020 Q3 2021 MW-32 (Class III) Chloride (mg/L) 35.99 36.3 Semi-Annually Quarterly 'l~ ~u ~-\'l Q2 2014 nn "' Notes: Highlighted text shows accelerated requirements resulting from Q2 2022 sampling event. Monitoring Well(Water Constituent Exceeding GWCL Class) Nitrate+ Nitrite (as N) (mg/L) Chloride (mg/L) MW-11 (Class II) Manganese (ug/L) Sulfate (mg/L) TDS (mg/L) MW-25 (Class TDS(mg/L) Ill) Nitrate+ Nitrite (as N) (mJVLl MW-26 Chloroform (ug/L) (Class Ill) Chloride (mJ?/Ll TDS (mi?/L) Nitrate+ Nitrite (ns N) (ml!/L) MW-30 Chloride (ml!/L) Selenium (ui?/L) (Class 11) TDS (mwL) Uranium (ui?/L) Nitrate + Nitrite (as N) {mJl/L} MW-31 Sulfate (mg/L) (Class Ill) TDS (mg/L) Uranium (ucl?/L) Chloride (mg/L) MW-12 Uranium (uwL) (Class II[) Selenium (ug/L) Bcr)'llium (ug/L) Cadmium (ug/L) Fluoride (111!1/L) MW-24 Nickel (mg/L) (Class nI) Manganese (ug/L) Thallium (ug/L) Gross Aloha (nf'i/L) Sulfate (mll/L) TDS (mwL) Field o~I (S.U.l MW-27 Nitrate+ Nitrite (as N) (mg/L) (Class Ill) Fluoride (mg/L) Chloride (mg/L) MW-28 Selenium (uWL) (Class II[) Nitrate+ Nitrite (as N) (ml!/L) Uranium (ug/L) MW-29 Uranium (ug/L) (Class Ill) MW-32 Chloride (mg/L) (Class Ill) Notes: NS= Not Required and Not Sampled NA= Not Applicable Exceedances are shown in yellow GWCLin Ql 2021 March 8, Sample 2021 Date GWDP 2.5 39.16 237 1/12/21 1309 2528 2976 1/11/21 0.62 70 1/14/21 58.31 3284.19 2.5 128 53.6 1/11/2 l 1918 9.82 5 993 2132 1/12/21 15 143 23.5 39 1/14/21 2 6.43 0.47 50 7507 1/14/21 2.01 7.5 2903 4450 5.03 -8.5 5.6 1/14/21 0.85 105 II.I 1/15/21 5 4.9 15 1/15/21 35.39 1/14/21 Ql 2021 Results February February March March 2021 2021 Q22021 Ql 2021 Monthly 2021 Monthly 2021 Sample Result Monthly Monthly Sample Sample Date Result Result Date Date Required Quarterly S)lmpling Wells 1.21 NA NA 46.4 46.4 185 2/9/21 254 3/8/21 221 04/20/21 1140 1260 1270 2010 2160 1950 2660 NS NA NS NA 04/14/21 0.619 0.764 0.617 2200 2/10/21 19.10 2190 04/21/2 l 57.4 71.3 3/9/21 63.9 3100 2700 3060 17.7 14.3 17.0 184 ~ 192 2/10/21 3/9/21 56.3 04/14/21 ---NA 10.2 17.1 14.3 17.4 1070 1130 1210 2460 2/9/21 2960 3/8/21 2400 04/13/21 19.7 22.2 20.2 354 380 388 Required Semiannual Sampling Wells 25.0 35.1 NS NA NS NA 4/20/21 2.75 NA NA 8.79 NA NA 0.916 NA NA 70.4 NA NA 7460 NS NA NS NA 4/29/2 l 2.74 NA NA 2.94 NA NA 2980 NA NA 4260 NA NA 5.08 NA NA 5.16 NS NA NS NA 4/15/21 NA 128 NA NA 14.0 NS NA NS NA 4/15/21 3.44 NA NA 10.3 NA NA 16.9 NS NA NS NA 4/14/21 36.9 NS NA NS NA 4/13/21 Table 3 -GWCL Exceedances under the March 8, 2021 GWDP Q2 2021 Results Q3 2021 Results Q4 2021 Results May2021 June2021 August August September September November November December December May 2021 June2021 Q32021 2021 Q42021 Q22021 Monthly Monthly Monthly Monthly Sample Q32021 Monthly 2021 2021 2021 Sample Q42021 2021 2021 2021 2021 Result Sample Sample Result Monthly Monthly Monthly Result Monthly Monthly Monthly Monthly Result Result Date Sample Date Date Date Result Sample Date Result Sample Date Result Sample Date Result Date Required Quarterly Sampling Wells Required Quarterly Sampling Wells Required Quarterly Sampling Wells 0.948 NA NA 0.924 NA NA 1.5 NA NA 47.7 46.4 52.1 48.3 57.0 49.6 52.8 53.6 53.9 237 5/10/21 NA 6/8/21 NA 7/27/21 376 8/10/21 NA 9/7/21 NA 10/20/21 286 11/16/21 261 12/13/21 300 1290 1280 1270 1470 1370 1240 1360 1300 1350 2110 2190 1960 2680 NA NA 2200 2230 2140 2720 NS NA NS NA 7/28/21 3100 NS NA NS NA 10/20/21 2680 11/16/21 2920 12/14/2 l 2590 1.42 1.06 0.368 0.352 1.42 0.710 0.928 I.IS 1.76 777 733 1590 723 996 516 540 568 1160 5/11/21 69.6 6/8/21 7/28/21 8/10/21 9/9/21 10/21/21 11/16/21 12/15/21 57.5 54.9 54.0 61.4 59.3 55.2 56.9 75.9 2790 NA NA 3390 NA NA 3010 3150 3130 17.7 18.6 17.0 20.6 16.5 15.4 14.3 18.0 18.6 162 188 170 188 161 183 182 182 184 55.7 5/ll/21 58.3 6/8/21 54.1 7/29/21 56.3 8/9/21 56.l 9/8/21 60.4 10/ 19/2 l 54.6 11/17/21 53.6 12/14/21 58.8 1580 NA NA 2010 NA NA 1790 1710 1610 10.3 10.7 9.84 9.60 9.38 9.74 9.76 9.67 JO.I 18.6 18.9 20.6 18.7 15.7 16.0 18.I 19.3 17.9 1170 1200 1170 1210 1130 1130 1220 1180 1220 2300 5/10/21 2610 6/7/21 2400 7/27/21 3100 8/9/21 2600 9/7/21 2870 10/19/21 2600 11/15/21 2610 12/13/21 2420 20.1 21.7 20.8 20.0 19.3 20.2 20.9 21.5 21.8 377 384 374 391 365 356 371 366 376 Required Semiannual Sampling Wells Required Semiannual Sampling Wells Required Semiannual Sampling Wells 22.9 22.2 NS NA NS NA 7/21/21 NS NA 28.8 32.4 23.1 NS NA 11/9/21 26.4 NS NA NS NA 2.78 NA NA 2.71 NA NA 2.66 NA NA 8.08 NA NA 9.26 NA NA 9.30 NA NA 0.925 NA NA 1.4 NA NA 0.988 NA NA 72.4 NA NA 76.7 NA NA 76.7 NA NA 7540 NS NA NS NA 7/29/21 7890 NS NA NS NA 11/10/21 7430 NS NA NS NA 3.02 NA NA 2.91 NA NA 3.14 NA NA 3.18 NA NA 1.92 NA NA 1.56 NA NA 2960 NA NA 3050 NA NA 3220 NA NA 4460 NA NA 4940 NA NA 4730 NA NA 5.00 NA NA 5.85 NA NA 5.23 NA NA 6.57 6.32 3.88 NS NA NS NA 7/22/21 NS NA NS NA 10/26/21 NS NA NS NA 0.69 NA 0.65 144 NA NA 152 NA NA 147 NA NA 13.4 NS NA NS NA 7/23/21 18.5 NS NA NS NA 10/26/21 11.2 NS NA NS NA 4.09 NA NA 6.09 NA NA 1.89 NA NA 8.52 NA NA 13.80 NA NA 6.03 NA NA 16.2 NS NA NS NA 7/22/21 15.8 NS NA NS NA 10/27/21 14.9 NS NA NS NA 31.8 NS NA NS NA 7/28/21 36.5 NS NA NS NA 11/2/21 36.1 NS NA NS NA Table 3-GWCL Exceedances under the March 8, 2021 GWDP Ql 2022 Results Q2 2022 Results February February Marcb 2022 March 2022 May 2022 May2022 June 2022 June 2022 Monitoring Well GWCL in March QI 2022 Ql 2022 2022 Monthly Q22022 Q2 2022 Monthly (Water Class) Constituent Exceeding GWCL 8,2021 GWDP Sample Date Result 2022 Monthly Monthly Sample Monthly Sample Date Result Monthly Monthly Sample Monthly Sample Date Result Date Result Sample Date Result Date Result Required Quarterly Sampling Wells Required Quarterly Sampling Wells Nitrate+ Nitrite (as N) (mg/L) 2.5 2.55 NA NA 2.2 1.6 l.9 Chloride (mg/L) 39.16 51.1 57.2 67.7 54.9 59.5 46.4 MW-II 1/18/22 156 2/8/22 233 3/8/22 224 4/18/22 5/4/22 254 6/6/22 228 (Class II) Manganese (ug/L) 237 180 Sulfate (mg/L) 1309 1020 1240 1170 1240 1270 866 TDS (mg/L) 2528 2050 1900 2080 2060 2290 2360 MW-25 (Class TDS (mg/L) 2976 l/17/22 2720 2/9/2022 2690 3/7/2022 2610 4/12/22 3600 5/3/2022 2660 6/7/2022 2730 III) Nitrate+ Nitrite (as N) (mg/L) 0.62 0.601 0.367 0.600 0.8 1.1 0.60 MW-26 Chloroform (ul!IL) 70 l/20/22 818 2/9/22 1580 3/8/22 1460 4/20/22 447 5/4/22 616 6/7/22 1250 (Class Ill) Chloride (mg/L) 58.31 77.1 58.6 64.1 56.8 63.2 47.4 TDS (me/L) 3284.19 3080 2980 2870 2560 2860 3120 Nitrate+ Nitrite (as N) (m2/L) 2.5 14.5 13.6 16.6 17 15 11.0 MW-30 Chloride (mg/L) 128 181 184 196 173 195 126 Selenium (u!l/L) 53.6 1/17/22 56.7 2/9/22 57.7 3/7/22 62.0 4/20/22 64.9 5/4/22 69.4 6/7/22 65.7 (Class II) TDS (mg/L) 1918 1680 1640 1500 1400 1640 1660 Uranium (ul!IL) 9.82 10.1 10.3 9.9 9.6 10.1 9.6 Nitrate+ Nitrite (as N) (mg/L) 5 18.0 13.5 17.0 18.0 13.0 /3.0 MW-31 Sulfate (m.l!/L) 993 1210 1250 731 l180 1220 1110 TDS (1112/L) 2132 1/19/22 2620 2/8/22 2680 3/7/22 2530 4/l 1/22 4300 5/3/22 2660 6/6/22 2690 (Class Ill) Uranium (ug/L) ts 21.7 22.1 22.5 22.0 22.9 21.5 Chloride (mg/L) 143 370 379 416 372 381 351 Required Semiannual Sampling Wells Required Semiannual Sampling Wells MW-12 Uranium (ug/L) 23.5 22.1 20.5 NS NS (Class Ill) l/20/22 NS NA NS NA 4/19/22 NA NA Selenium (ug/L) 39 25.6 31.3 Beryllium (ug(L) 2 2.71 NA NA 2.5 NA NA Cadmium (u!?,/L) 6.43 8.46 NA NA 9.20 NA NA Fluoride (m!?,/L) 0.47 1 NA NA 0.8 NA NA MW-24 Nickel (111!!/L) 50 80.9 NA NA 74.3 NA NA (Class Ill) Man,l!OMSC (uQ/L) 7507 1/27/22 7630 NS NA NS NA 4/27/22 7070 NS NA NS NA Thallium (u!!.IL) 2.01 2.66 NA NA 3.1 NA NA Gross Aloha (oCi/L) 7.5 2.26 NA NA 2.28 NA NA Sulfate (mg/L) 2903 3060 NA NA 3120 NA NA TDS (mg/L) 4450 4140 NA NA 3350 NA NA Field oH (S.U.) 5.03 -8.5 5.31 NA NA 4.81 NA NA MW-27 Nitrate+ Nitrite (as N) (mg/L) 5.6 6.25 6.30 (Class Ill) l/l 8/22 NS NA NS NA 4/12/22 NS NA NS NA Fluoride (mg/L) 0.85 NA 0.90 Chloride (mg/L) 105 140 NA NA 130 NA NA MW-28 Selenium (ug/L) I I. I l/20/22 13.3 NS NA NS NA 4/19/22 19.8 NS NA NS NA (Class III) Nitrate+ Nitrite (as N) (mg/L) 5 4.03 NA NA 5.1 NA NA Uranium (ug/L) 4.9 8.50 NA NA JO.JO NA NA MW-29 Uranium (ug/L) 15 l/18/22 15.1 NS NA NS NA 4/14/22 15.7 NS NA NS NA (Class II[) MW-32 Chloride (mg/L) 35.39 1/19/22 35.0 NS NA NS NA 4/11/22 28.6 NS NA NS NA (Class Ill) Pursuant to the DWMRC letter Ot February 2, 202·2, these constituents-will no tonger be monitored on an ~cceterated schedule. These constltuen~~ will be dropped from this report after this quarter. Tab A Site Plan and Perched Well Locations White Mesa Site TW4-43 temporary perched monitoring well ~ installed September, 2021 TWN-20 temporary perched nitrate monitoring C well installed April, 2021 MW-24A perched monitoring well installed • December 2019 TW4-42 ¢ temporary perched monitoring well installed April 2019 TW4-40 perched chloroform pumping well EB installed February 2018 TW4-19 perched chloroform or EB nitrate pumping well MW-38 -¢-perched monitoring well installed February 2018 MW-5 • perched monitoring well TW4-12 0 temporary perched monitoring well TWN-7 temporary perched nitrate monitoring 0 well PIEZ-1 perched piezometer "1 RUIN SPRING b seep or spring HYDRO GEO CHEM, INC. iv£.20~ Celt2 • I\IV€30 WHITE MESA SITE PLAN SHOWING LOCATIONS OF PERCHED WELLS AND PIEZOMETERS APPROVED DATE REFERENCE H:/718000/may22/Uwelloc0322.srf FIGURE A-1 TabB Field Data Worksheets Quarterly Sampling Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-01 Sampling Prog_ram Field Sample ID MW-01 04142022 Sampling_ Event 2022 Q2 GW Quarterly Purge Date & Time 4/14/2022 6:45 Sample Date & Time 4/14/2022 9:45 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) -4 Purging Method 2 Casings Previous Well Sampled MW-18 Casing Volume (gal) 19.48 Calculated Casing Volumes Purge Duration (min) 179.61 pH Buffer 7 .0 7.0 Well Depth (ft) 118.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 3 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 64.90 Conductivity Dissolved Date/Time Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/14/2022 9:42 38.40 1712 7.23 14.16 266 0 11.9 4/14/2022 9:43 38.62 1746 7.22 14.12 259 0 11.0 4/14/2022 9:44 38.84 1731 7.20 14.10 255 0 11.2 4/14/2022 9:45 39.06 1730 7.19 14.16 252 0 10.5 Pumping Rate Calculations jvolume ~f_ water purged (gals) 39.06 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 180.00 jFinal Depth to Water (feet) 97.15 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory GEL Anal}'t_ical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Gross Alpha y WATER 1 250-ml HOPE y HN03 y Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Comments: I Arrived on site at 0642. Purge be_gan at 0645. Purged well for a total of 180 minutes. Purge ended and samples collected at 0945. Water was clear. Left site at 0955. Signature of Field Technician ~=~ ....... M~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-02 Sampling P!ogram Field Sample ID MW-02 04122022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/12/2022 11:35 Sample Date & Time 4/12/2022 13:35 [sampler TH/DL Purging Equipment Pump Weather Conditions Cloudy Pump Type QED External Ambient Temperature (C) 5 Purging Method 2 Casings Previous Well Sampled MW-25 Casing Volume (gal) 12.79 Calculated Casing Volumes Purge Duration (min) 117.96 pH Buffer 7.0 7.0 Well Depth (ft) 128.80 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 109.20 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4/12/2022 13:32 25.38 3686 7.10 13.37 323 0 3.5 4/12/2022 13:33 25.60 3676 7.11 13.78 323 0 3.2 4/12/2022 13:34 25.82 3677 7.12 13.85 323 0 3.2 4/12/2022 13:35 26.04 3678 7.12 13.82 323 0 3.2 Pumping Rate Calculations [vol_u_rne of water purged (gals) 26.04 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 120.00 [Final Depth to Wate_,Jfeet) 117.75 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 {pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 DegC y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: [ Arrived on sit_E,_ at 1_ 132. Purge_ b_e_g_an at 1135. Purged well for a total of 120 minute~. Purge ended and samples collected at 1335. Water was clear. Left site at 1345. Signature of Field Technician -.:3 ....... ~-h-~~~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-03a Sampling Program Sampling Prog_ram Field Sample ID MW-03A 04272022 Sampling Event Sampling Event 2022 Q2 GW Quarterly 2022 Q2 GW Quarterly Purge Date & Time 4/26/2022 7:00 Sample Date & Time 4/27/2022 9:15 !sampler !sampler I TH/DL TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 4 Purging Method 2 Casings Previous Well Sampled MW-22 Casing Volume (gal) 7.16 Calculated Casing Volumes Purge Duration (min) 68.94 pH Buffer 7.0 7.0 Well Depth (ft) 95.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 84.02 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/26/2022 8:10 14.56 5655 7.00 14.65 368 1.2 76.0 4/27/2022 9:14 5802 6.81 14.62 Before 4/27/2022 9:23 5785 6.83 14.65 After jvolume of water purged (gals) Pumping_ Rate Calculations 14.56 Flow Rate (Q = S/60) (gal/min) .208 Time to evacuate 2 Casing Volumes (min) 70.00 §nal Depth to Water (feet) 92.03 Number of casing Volumes 2.00 Volume, if well evacuated to dryness O 14.56 Name of Certified Analytical Laboratory AWSL Analytical Sameles Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4DegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: Arrived on site at 0655. Purge began at 0700. Purged well for a total of 70 minutes. Purged well dry. Purge ended at 0810. Water was clear. Left site at 0812. Arrived on site at 091 2. Depth to water was 85.40. Samples bailed and collected at 0915. Left site at 0926. Signature of Field Technician ~~~ I Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-05 Sampling Program Field Sample ID MW-05 04182022 Sampling_ Event 2022 Q2 GW Quarterly Purge Date & Time 4/18/2022 11:35 Sample Date & Time 4/18/2022 15:00 [sampler TH/DL Purging Equipment Pump Weather Conditions Cloudy and windy Pump Type QED External Ambient Temperature (C) 17 Purging Method 2 Casings Previous Well Sampled MW-17 Casing Volume (gal) 21.82 Calculated Casing Volumes Purge Duration (min) 201.13 pH Buffer 7.0 7.0 Well Depth (ft) 141.50 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 108.08 Conductivity Dissolved Date/Time Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/18/2022 14:47 43.83 2794 7.34 15.65 312 0 6.4 4/18/2022 14:58 44.05 2798 7.31 15.70 309 0 6.8 4/18/2022 14:59 44.26 2808 7.29 15.66 307 0 6.7 4/18/2022 15:00 44.48 2797 7.29 15.40 303 0 6.7 Pumping Rate Calculations [volume of water purged (gals} 44.48 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 205.00 jFinal Depth to Water (feet) 125.86 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 DegC y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: I Arrived on site at 1132. Purge began at 1135. Purg~_d well for~ total of 205 minutes. PlJ_r_g_e ended and samples collected at 1500. Water was clear. Left site at 1511 . Signature of Field Technician ~,,._r~-ry-~...c,. Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-11 Sampling Program Field Sample ID MW-11 04182022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/18/2022 6:50 Sample Date & Time 4/18/2022 11:20 I sampler I TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 5 Purging Method 2 Casings Previous Well Sampled MW-23 Casing Volume (gal) 29.25 Calculated Casing Volumes Purge Duration (min) 269.62 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 85.20 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/18/2022 11:17 57.93 2980 7.36 14.52 336 41.0 0 4/18/2022 11:18 58.15 2975 7.37 14.55 335 43.0 0 4/18/2022 11:19 58.37 2978 7.37 14.57 334 45.0 0 4/18/2022 11:20 58.59 2990 7.37 14.53 333 46.0 0 Pumping Rate Calculations ~olume of water purged (gals) 58.59 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 270.00 !Final Depth to Water (feet) 85.83 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Anal~ical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2504 (pH <2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: Arrived on site at 0645. Purge began at 0650. Purged well for a total of 270 minutes. Purge ended and samples collected at 1120. Water was mostly clear with tiny little bubbles surfacing. Left site at 1130. Signature of Field Technician ~=~-Md~ I Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-12 Sampling Program Sampling_ Program Field Sample ID MW-12 04192022 Sampling Event Sampling Event 2022 Q2 GW Quarterly 2022 Q2 GW Quarterly Purge Date & Time 4/19/2022 7:15 Sample Date & Time 4/19/2022 9:25 !sampler [sampler I TH/DL TH/DL Purging Equipment Pump Weather Conditions Cloudy Pump Type QED External Ambient Temperature (C) 10 Purging Method 2 Casings Previous Well Sampled MW-14 Casing Volume (gal) 13.71 Calculated Casing Volumes Purge Duration (min) 126.38 pH Buffer 7.0 7.0 Well Depth (ft) 130.40 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 109.40 Conductivity Dissolved Date!Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4/19/2022 9:22 27.55 4080 6.70 14.69 323 0 16.0 4/19/2022 9:23 27.77 4074 6.65 14.56 322 0 15.0 4/19/2022 9:24 27.99 4084 6.62 14.78 322 0 15.0 4/19/2022 9:25 28.21 4079 6.62 14.75 322 0 14.5 Pumping Rate Calculations [\/olume of water purged (gals) 28.21 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 130.00 [ Final Depth to Water (feet) 122.25 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analyt_ical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: Arrived on site at 0710. Purge began at 0715. Purged well for a total of 130 minutes. Purged well for a total of 130 minutes. Purge ended and samples collected at 0925. Water was clear. Left site at 0935. Signature of Field Technician ~c.u'.J<""-"C....-,./-,r,:,.~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan ,/ White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-14 Sampling__J>_r_ogram Field Sample ID MW-14_04182022 Sampling Event 2022 Q2 GW Quarterly Purg_e Date & Time 4/18/2022 12:10 Sample Date & Time 4/18/2022 15:00 [sampler TH/DL Purging Equipment Pump Weather Conditions Cloudy and windy Pump Type QED External Ambient Temperature (C) 20 Purging Method 2 Casings Previous Well Sampled MW-05 Casing Volum~ (gal) 17.69 Calculated Casing Volumes Purge Duration (min) 163.09 pH Buffer 7.0 7.0 Well Depth (ft) 128.70 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 101.60 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/18/2022 14:57 36.23 3846 6.56 15.00 318 0 1.0 4/18/2022 14:58 36.45 3850 6.55 14.93 318 0 1.1 4/18/2022 14:59 36.67 3838 6.55 14.95 319 0 1.2 4/18/2022 15:00 36.89 3838 6.55 14.94 319 0 1.2 Pumping Rate Calculations [Volume of wa_t~r purged (gals) 36.89 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 170.00 I Final Depth to Water (feet) 101.90 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-mLHDPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: [ Ar~ved on site at 1206. Purge began at 1210. Pu~g_ed well for a total of 1__70 minutes. Purg_e ended and samples collected at 1500. Water was clear. Left site at 1510. Signature of Field Technician ~"-'-"~#~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-15 Sampling Program Sampling Program Field Sample ID MW-15 04192022 Sampling Event Sampling Event 2022 Q2 GW Quarterly 2022 Q2 GW Quarterly Purge Date & Time 4/19/2022 7:25 Sample Date & Time 4/19/2022 10:45 !sampler !sampler I TH/DL TH/DL I Purging Equipment Pump Weather Conditions Cloudy and windy Pump Type QED External Ambient Temperature (C) 10 Purging Method 2 Casings Previous Well Sampled MW-12 Casing Volume (gal) 20.79 Calculated Casing Volumes Purge Duration (min) 191.68 pH Buffer 7 .0 7.0 Well Depth (ft) 137.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 105.15 Conductivity Dissolved Date/Time Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/19/2022 10:42 42.74 4212 6.83 15.00 324 0 20.3 4/19/2022 10:43 42.96 4220 6.81 15.01 324 0 20.0 4/19/2022 10:44 43.18 4222 6.81 14.95 324 0 19.0 4/19/2022 10:45 43.40 4225 6.82 14.96 325 0 18.9 Pumping Rate Calculations [volume of water purged (gals) 43.40 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 200.00 [Final Depth to Water (feet) 107.60 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: I Arrived on site at 0720. Purge began at 0725. Purged well for a total of 200 minutes. Purge ended and samples collected at 1045. Water was clear. Left site at 1055. Signature of Field Technician ..=3~.-hi Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-17 Sampling Program Field Sample ID MW-17 04182022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/18/2022 7:25 Sample Date & Time 4/18/2022 11:55 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 5 Purging Method 2 Casings Previous Well Sampled MW-11 Casing Volume (gal) 26.03 Calculated Casing Volumes Purge Duration (min) 239.95 pH Buffer 7.0 7.0 Well Depth (ft) 112.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 72.13 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/18/2022 11:52 57.93 3644 6.96 15.05 329 4.0 2.0 4/18/2022 11:53 58.15 3651 6.94 15.10 329 4.5 3.0 4/18/2022 11:54 58.37 3656 6.94 15.01 329 4.6 4.0 4/18/2022 11:55 58.59 3652 6.94 15.05 330 4.7 4.2 Pumping Rate Calculations - [volume of water purged (gals) 58.59 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 270.00 [Final Depth to Water (feet) 86.65 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: { Arrived or1_sile at 0720. Purge began at 0725. Purged well for a total of 27_9 minutes. Purge ended and samples collected at 1155. Water was clear. Left site at 1205. Signature of Field Technician ~=~-M~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan a_-,~l r ,· ' ., -.'"· /•_l 'L /~Y~~c;:- White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-18 Sampling Program Sampling Program Field Sample ID MW-18 04132022 Sampling Event Sampling Event 2022 Q2 GW Quarterly 2022 Q2 GW Quarterly Purge Date & Time 4/13/2022 5:25 Sample Date & Time 4/13/2022 11:35 I sampler !sampler I TH/DL TH/DL I Purging Equipment Pump Weather Conditions Cloudy Pump Type QED External Ambient Temperature (C} -3 Purging Method 2 Casings Previous Well Sampled MW-19 Casing Volume (gal) 39.31 Calculated Casing Volumes Purge Duration (min) 362.309 pH Buffer 7.0 7.0 Well Depth (ft} 134.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos} 1000 Depth to Water Before Purging (ft) 73.80 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm} pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/13/2022 11:32 79.63 3199 6.55 16.30 324 0 0 4/13/2022 11:33 79.85 3257 6.56 16.35 323 0 0 4/13/2022 11:34 80.07 3232 6.57 16.40 322 0 0 4/13/2022 11:35 80.29 3230 6.57 16.30 322 0 0 Pumping Rate Calculations [volume of wat~r purged (gals) 80.29 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 370.00 !Final Depth to Water (feet) 74.82 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical ~_mples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: I Arrived on site at 0522. Purge began at 0525. Purg~d _well for a total of 37'0 minutes. Purge ended and samples collected at 1135. Water was clear. Left site at 1145. Signature of Field Technician ~"""v,,,~-rA~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan e-~ · l · r / /; . .-Y~eFTS ~. ~ . . ~~ White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-19 Sampling Program Field Sample ID MW-19 04132022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/13/2022 5:15 Sample Date & Time 4/13/2022 13:35 !sampler I TH/DL I Purging Equipment Pum p Weather Conditions Cloudy Pump Type QED External Ambient Temperature (C) -3 Purging Method 2 Casings Previous Well Sampled MW-35 Casing Volume (gal) 54.10 Calculated Casing Volumes Purge Duration (min) 498.62 pH Buffer 7.0 7.0 Well Depth (ft) 149.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 66.15 Conductivity Dissolved DatefTime Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/13/2022 13:32 107.84 1346 6.92 15.40 311 0 124.0 4/13/2022 13:33 108.06 1345 6.92 15.15 312 0 124.0 4/13/2022 13:34 108.28 1349 6.92 15.20 312 0 123.0 4/13/2022 13:35 108.50 1316 6.92 15.10 313 0 125.0 Pumping Rate Calculations [volume of water purged (gals) 108.50 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 500.00 §.al_ Depth to Water (feet) 82.14 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical ~amples Information Sample Container Preservative Type of Sample/ Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2504 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: I Arrived on site at 0512. Purge began at 0515. Purged well !<:Jr ~!al of 500 minutes. Pu!ge ended and samples collected at 1335. Water was clear. Left site at 1345. Signature of Field Technician ~Lu"JLP~h Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-20 Sampling Program Field Sample ID MW-20 05172022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/26/2022 12:27 Sample Date & Time 5/17/2022 8:00 !sampler I TH/DL Purging Equipment Bailer Weather Conditions Cloudy Pump Type Grundfos External Ambient Temperature (C) 18 Purging Method 2 Casings Previous Well Sampled MW-24 Casing Volume (gal) 5.06 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 92.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 84.25 Conductivity Dissolved Date/Time Gallons Purged (umhos/cm) pH (pH Units) Temp {deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4/26/2022 12:34 6291 5.84 15.25 520 16.6 83.0 5/17/2022 7:59 5485 7.70 16.40 Before 5/17/2022 8:07 5499 7.64 16.32 After Pumping Rate Calculations [volume of water purged (g_als) 8.00 Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () [ Final Depth to Water {feet) 92.00 Number of casing Volumes 1.58 Volume, if well evacuated to dryness (gals} 8.00 Name of Certified Analyt_ical Laboratory AWSL Analytical S~rn_ples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: Arrived on site at 1224. Bailing began at 1227. Bailed a total of 8 gallons from well. Bailed well dry. Water was a little murky. Bailing ended at 1237. Left site at 1239. Arrived on site at 0756. Depth to water was 89.30. Samples bailed and collected at 0800. Left site at 0810. Signature of Field Technician ~(v~ ~ I Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan e -. F-:'·' .. -~· .-,;. -' •f ~.,. /• },···· .·'~y~,s- White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-22 Sampling Program Field Sample ID MW-22_04252022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/25/2022 7:50 Sample Date & Time 4/25/2022 12:50 !sampler I TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 6 Purging Method 2 Casings Previous Well Sampled MW-36 Casing Volume (gal) 31.16 Calculated Casing Volumes Purge Duration (min) 287.19 pH Buffer 7.0 7.0 Well Depth (ft) 114.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 66.28 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4/25/2022 12:47 64.44 7580 4.56 15.30 407 140.3 11.0 4/25/2022 12:48 64.66 7551 4.58 15.38 416 145.0 11.0 4/25/2022 12:49 64.88 7557 4.58 15.27 422 148.0 10.7 4/25/2022 12:50 65.10 7557 4.58 15.23 426 151.0 10.5 jvolume of water purged (gals) Pumping_ Rate Calculations 65.10 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 300.00 [Final Depth to Water (feet) 98.40 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical _S~ll'lples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 {pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI {pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: Arrived on site at 07 46. Purge began at 0750. Purged well for a total of 300 minutes. Purge ended and samples collected at 1250. Water was mostly clear with tiny little bubbles surfacing . Left site at 1300. Signature of Field Technician ..:=:i~_.cc--h'l.a-'~ I Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan e ·~· '---. · /r --· ... ~~y,,,,...-,.... s .... J.J!!!!!!!!! - White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-23 Sampling Program Field Sample ID MW-23 04272022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/26/2022 0:00 Sample Date & Time 4/27/2022 8:40 I sampler I TH/DL Purging Equipment Pump Weather Conditions Cloudy Pump Type QED External Ambient Temperature (C) 17 Purging Method 2 Casings Previous Well Sampled Casing Volume (gal) 11.95 Calculated Casing Volumes Purge Duration (min) 114.90 pH Buffer 7.0 7.0 Well Depth (ft) 132.00 pH Buffer 4.0 4.0 Well Casing Diameter () 4 Specific Conductance () 1000 Depth to Water Before Purging (ft) 113.70 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4/14/2022 14:30 24.96 3795 6.74 14.90 305 2.5 43.5 4/27/2022 8:39 3829 6.27 14.11 Before 4/27/2022 8:47 3826 6.30 14.10 After @:olume of wate_r purged () Pumping Rate Calculations 24.96 Flow Rate (Q = S/60) (gal/min) 0.208 Time to evacuate 2 Casing Volumes (min) 105.00 !Final Depth to Water (feE!t) 128.15 Number of casing Volumes 2.00 Volume, if well evacuated to dryness (gals) 21.84 Name of Certified Analytical Laboratory_ AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: Arrived on site at 1227. Purge began at 1230. Purged welffor a total of 120 minutes. Purged well dry. Purge erided at 1430. Water was clear. Left site at 1431. Arrived on site at 0835. Depth to water was 120.44. Samples collected at 0840. Left site at 0851 . Signature of Field Technician I Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan ~~ -~-~-,·'~ ~YFY'f'FTS White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-24 Sampling Program Field Sample ID MW-24 04272022 Sampling Event 2022 Q2 GW Quarterly I Purge Date & Time 4/26/2022 11:50 Sample Date & Time 4/27/2022 8:00 !sampler I TH/DL I Purging Equipment Bailer Weather Conditions Cloudy Pump Type Grundfos External Ambient Temperature (C) 17 Purging Method 2 Casings Previous Well Sampled MW-24A Casing Volume (gal) 6.73 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 120.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 109.68 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxyg_en (%) Before/After 4/26/2022 12:01 6.00 4421 4.61 15.08 554 98.0 0 4/27/2022 8:00 4427 4.80 14.41 Before 4/27/2022 8:05 4430 4.81 14.35 After Pump_i_l!_g_ Rate Calculations !Volume of water purged (gals) 14.00 Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () I Final Depth to Water (feet) 120.00 Number of casing Volumes 2.00 Volume, if well evacuated to dryness (gals) 14.00 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 DegC y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: Arrived on site at 1150. Bailing began at 1153. Bailed a total of 14 gallons from well. Bailed well dry. Water was dirty. Left site at 1213. Arrived on site at 0756. Depth to water was 09.56. Samples bailed and collected at 0800. Left site at 0806. Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan E!F-:_-.,· , .. · ,,_.-;, ! ··1 ' _,_, /L~~ " .'~Y~--Z$ '__ .,,'.JI· •. · _t' White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-24A Sampling Program Field Sample ID MW-24A 04272022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/26/2022 8:25 Sample Date & Time 4/27/2022 7:40 !sampler I TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 10 Purging Method 2 Casings Previous Well Sampled MW-03A Casing Volume (gal) 7.33 Calculated Casing Volumes Purge Duration (min) 70.57 pH Buffer 7.0 7.0 Well Depth (ft) 122.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 110.76 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/26/2022 9:40 15.60 4410 5.00 14.24 388 2.9 90.6 4/27/2022 7:39 4401 4.75 15.40 Before 4/27/2022 7:47 4410 4.79 15.29 After Pumpi~g_ Rate Calculations !Volume of water purged (gals) 15.60 Flow Rate (Q = S/60) (gal/min) .208 Time to evacuate 2 Casing Volumes (min) 75.00 I Final Depth to Water (feet) 119.97 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 15.60 Name of Certified Analytical Laboratory GEL Anal~ical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Gross Alpha y WATER 1 250-ml HDPE y HN03 y Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Comments: Arrived on site at 0821 . Purge began at 0825. Purged well for a total of 75 minutes. Purged well dry. Purge ended at 0940. Water was clear. Left site at 0942. Arrived on site at 0736. Depth to water was 110.64. Samples collected at 07 40. Left site at 0750. I Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-25 Sampling_ Program Field Sample ID MW-25 04122022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/12/2022 7:25 Sample Date & Time 4/12/2022 10:55 [sampler TH/DL Purging Equipment Pump Weather Conditions Cloudy and windy Pump Type QED External Ambient Temperature (C} 4 Purging Method 2 Casings Previous Well Sampled MW-27 Casing Volume (gal} 22.13 Calculated Casing Volumes Purge Duration (min} 204.02 pH Buffer 7.0 7.0 Well Depth (ft} 115.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 81.10 Conductivity Dissolved Date/Time Gallons Purged (gal} (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV} Turbidity (NTU) Oxygen(%} Before/ After 4/12/2022 10:52 44.91 3146 6.73 14.96 332 0 0 4/12/2022 10:53 45.13 3130 6.72 14.90 332 0 0 4/12/2022 10:54 45.35 3145 6.71 14.79 331 0 0 4/12/2022 10:55 45.57 3131 6.71 14.70 331 0 0 @::olume of V\f_ater purged (gals} Pumpin_g_ Rate Calculations 45.57 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 [Final Depth t<> Water (feet) 83.06 Number of casing Volumes 2.00 Volume, if well evacuated to dryness() 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 DegC y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: I Arrived on site at 0722. Purge began at 072~5.J:>urged well for a total o~ O minutes. Purge ended and samples collected at 1055. Water was clear. Left site at 1104. Signature of Field Technician 2>,D~~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan S ·~·· . , . ,/r--. ~. r--I" .I "'"' ~--,=;, .~Y~S "'. '.I White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-26 Sampling Program Field Sample ID MW-26 04202022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/20/2022 13:59 Sample Date & Time 4/20/2022 14:00 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny and windy Pump Type Grundfos External Ambient Temperature (C) 21 Purging Method 2 Casings Previous Well Sampled MW-30 Casing Volume (gal) 28.14 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 121.33 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 78.23 Conductivity Dissolved Date/Time Gallons Purged (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4/20/2022 14:00 3290 6.70 16.70 288 1.0 39.0 Pumping Rate Calculations -!volume of water purged O Flow Rate (Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes () !Final Depth to Water (feet) 99.45 Number of casing Volumes Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soi Ids y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI {pH<2), 4 Deg C y Nutrients y WATER 1 250-mLHDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: [ Arrived on site at 1356. Samples collected at 1400. Water was clear. Left site at 1406. Signature of Field Technician Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-26 Sampling_ Program Field Sample ID MW-26 04272022 Sampling Event Q2 2022 MW-26 Resample Purge Date & Time 4/27/2022 9:45 Sample Date & Time 4/27/2022 9:45 !sampler TH/DL Purging Equipment Pump Weather Conditions Cloudy Pump Type Grundfos External Ambient Temperature (C) 19 Purging Method 2 Casings Previous Well Sampled MW-38 Casing Volume (gal) 28.79 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 121.33 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 77.23 Dissolved Date/Time Gallons Purged Conductivity (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/27/2022 9:45 3333 6.74 15.06 336 0 23.4 Pumping Rate Calculations [volume of ~ater purged () Flow Rate (Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes () [Final Depth to Water (feet) 88.84 Number of casing Volumes Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory GEL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number I Type Sample Filtered? Type I Added? Gross Alpha y WATER 1 T 250-ml HOPE y HN03 I y Comments: [ Arrived on site at 0940. Samples collected at 0945. Water was clear. Left site at 0948. Signature of Field Technician Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-27 Sampling Program Field Sample ID MW-27 04122022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/12/2022 7:15 Sample Date & Time 4/12/2022 11:15 !sampler I TH/OL I Purging Equipment Pump Weather Conditions Cloudy and windy Pump Type QED External Ambient Temperature (C) 4 Purging Method 2 Casings Previous Well Sampled MW-32 Casing Volume (gal) 24.48 Calculated Casing Volumes Purge Duration (min) 225.69 pH Buffer 7.0 7.0 Well Depth (ft) 95.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 57.50 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4/12/2022 11:12 51.42 1240 7.36 14.66 306 0 95.0 4/12/2022 11:13 51.64 1239 7.37 14.62 304 0 95.7 4/12/2022 11:14 51.86 1240 7.37 14.58 305 0 95.3 4/12/2022 11:15 52.08 1240 7.37 14.60 304 0 95.2 [volume of water purged (gals) Pumpin_g Rate Calculations 52.08 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 240.00 [ Final Depth to Water (feet) 58.93 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: I Arrived on site at 0712. Purge began at 0715. Purged well for a total of 240 minutes. Pu rge ended and samples collected at 1115. Water was clear. Left site at 1125. Signature of Field Technician -:3(.V~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-27 Sampling Program Field Sample ID MW-27 05162022 Sampling Event Q2 2022 TDS Resample Purge Date & Time 5/16/2022 9:55 Sample Date & Time 5/16/2022 11:50 [sampler TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 18 Purging Method 2 Casings Previous Well Sampled MW-32 Casing Volume (gal) 24.01 Calculated Casing Volumes Purge Duration (min) 221.35 pH Buffer 7.0 7.0 Well Depth (ft) 95.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 58.22 Dissolved Date/Time Gallons Purged (gal) Conductivity (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 5/16/2022 11:47 49.25 1192 7.45 15.36 349 1.0 96.2 5/16/2022 11:48 49.47 1192 7.45 15.21 347 1.0 97.5 5/16/2022 11:49 49.69 1192 7.45 15.28 349 1.0 96.8 5/16/2022 11:50 49.91 1192 7.45 15.26 349 1.0 96.8 Pumping Rate Calculations [volume <>!_water purged (gal~) 49.91 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 230.00 [Final Depth to Water (feet) 59.66 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory_ AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number I Type Sample Filtered? Type I Added? Total Dissolved Soilds y WATER 1 I 250-ml HOPE u 4 Deg C I y Comments: I Arrived on site at 0755. Purge began at 0800. PUl'g_ed well for a total ol 2::l() minutes. Purge ended and sample collected at 1150. Water was clear. Left site at 1154. Signature of Field Technician ._:3...,vv~-a"~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-28 Sampling Program Field Sample ID MW-28 04192022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/19/2022 11:05 Sample Date & Time 4/19/2022 14:45 lsameler TH/DL Purging Equipment Pump Weather Conditions Cloudy and windy Pump Type QED External Ambient Temperature (C) 17 Purging Method 2 Casings Previous Well Sampled MW-40 Casing Volume (gal) 23.31 Calculated Casing Volumes Purge Duration (min) 214.85 pH Buffer 7.0 7.0 Well Depth (ft) 110.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 74.30 Conductivity Dissolved Date/Time Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/19/2022 14:42 47.08 4067 6.20 15.70 338 1.2 29.4 4/19/2022 14:43 47.30 4074 6.22 15.67 337 1.2 30.0 4/19/2022 14:44 47.52 4065 6.24 15.60 336 1.1 29.0 4/19/2022 14:45 47.74 4071 6.24 15.65 336 1.2 28.0 Pumping Rate Calculations [volume of water purged (gals) 47.74 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 220.00 [Final Depth to Wat~(feet) 77.16 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2). 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: [ Arrived on site at 1101. Purge bega_!l at 1105. Purged well for a total 220 minute~_purge ended and samples collected at 1445. Water was clear. Left site at 1455. Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-29 Sampling Program Field Sample ID MW-29 04142022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/14/2022 6:55 Sample Date & Time 4/14/2022 10:05 !sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) -4 Purging Method 2 Casings Previous Well Sampled MW-01 Casing Volume (gal) 18.38 Calculated Casing Volumes Purge Duration (min) 169.41 pH Buffer 7.0 7.0 Well Depth (ft) 135.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 106.85 Conductivity Dissolved Date/Time Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/14/2022 10:02 40.57 4533 6.52 14.21 268 9.2 1.3 4/14/2022 10:03 40.79 4548 6.53 14.23 267 9.2 1.1 4/14/2022 10:04 41.01 4548 6.52 14.21 267 9.3 1.2 4/14/2022 10:05 41.23 4543 6.52 14.19 266 9.3 1.2 Pumping Rate Calculations [yolu_r11e of water pllrged (gals) 41.23 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 190.00 [ Final Deeth to Water (feet) 109.40 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: [ Arrived on site at 0652. P_urge began at 0655. Purged well for a total of 190 minutes. Pu~ge e_ri_ded and samples collected at 1005. Water was clear. Left site at 1020. Signature of Field Technician ~UA,I~~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-30 Sampling Program Field Sample ID MW-30 04202022 Sampling_ Event 2022 Q2 GW Quarterly Purge Date & Time 4/20/2022 7:40 Sample Date & Time 4/20/2022 11:40 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 9 Purging Method 2 Casings Previous Well Sampled MW-39 Casing Volume (gal) 22.88 Calculated Casing Volumes Purge Duration (min) 210.94 pH Buffer 7.0 7.0 Well Depth (ft) 110.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 74.95 Conductivity Dissolved DatefTime Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4/20/2022 11:37 51.42 2187 6.90 15.30 299 0 0 4/20/2022 11:38 51.64 2191 6.91 15.20 300 0 0 4/20/2022 11:39 51.86 2196 6.92 15.13 300 0 0 4/20/2022 11:40 52.08 2202 6.92 15.87 301 0 0 Pumping Rate Calculations [volume of water pur9ed (gals) 52.08 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 240.00 [Final Depth to Water (feet) 76.02 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analyt_ical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: ~rrived on sit~0735. Purge beg___?n at 0740. PurgEl_d w~II for a total of 240 minutes. Purge ended and samples collected at 1140. Water was clear. Left site at 1150. Signature of Field Technician -2> .... ~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-31 Sampling Program Field Sample ID MW-31 04112022 Sampling_ Event 2022 Q2 GW Quarterly Purge Date & Time 4/11/2022 7:35 Sample Date & Time 4/11/2022 13:45 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 6 Purging Method 2 Casings Previous Well Sampled N/A Casing Volume (gal) 39.78 Calculated Casing Volumes Purge Duration (min) 366.64 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 69.08 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4/11/2022 13:42 79.63 3326 6.98 15.15 268 0 112.0 4/11/2022 13:43 79.85 3358 6.97 15.00 268 0 111.2 4/11/2022 13:44 80.07 3355 6.99 14.98 269 0 111.2 4/11/2022 13:45 80.29 3360 6.98 14.92 269 0 111.0 Pumei11_g Rate Calculations [volLJme of water purged (gals) 80.29 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 370.00 !Final Depth to Water (feet) 70.86 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/ Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: [ Arrived on site at 0730. Purge began at 0735. Purged well for a total of 370 minutes. Purge ended and samples collected at 1345. Water was clear. Left site at 1355. Signature of Field Technician ~ ·' -->~' Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-32 Sampling Program Field Sample ID MW-32 04112022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/11/2022 7:45 Sample Date & Time 4/11/2022 12:45 !sampler I TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 6 Purging Method 2 Casings Previous Well Sampled MW-31 Casing Volume (gal) 31.61 Calculated Casing Volumes Purge Duration (min) 291.35 pH Buffer 7.0 7.0 Well Depth (ft) 130.60 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 82.19 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/11/2022 12:42 64.44 3677 6.50 15.00 294 94.0 19.4 4/11/2022 12:43 64.66 3637 6.55 14.90 285 95.0 18.0 4/11/2022 12:44 64.88 3639 6.52 14.85 283 98.0 17.0 4/11/2022 12:45 65.10 3642 6.51 14.82 281 99.0 17.0 Pumping_ Rate Calculations !volume of water p_t.Jrged (gals) 65.10 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 300.00 I Final De~th to Water (feet) 85.63 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analyti~ S~mples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: Arrived on site at 0742. Purge began at 0745. Purged well tor a total of 300 minutes. Purge ended and samples collected at 1245. Water was a little murky with little bubbles surfacing. Left site at 1255. Signature of Field Technician ~~)~ I Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-32 Sampling. Program Field Sample ID MW-32 05162022 Sampling Event Q2 2022 TDS Resample Purge Date & Time 5/16/2022 7:20 Sample Date & Time 5/16/2022 12:20 !sampler TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 17 Purging Method 2 Casings Previous Well Sampled N/A Casing Volume (gal) 31.40 Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 7.0 Well Depth (ft) 130.60 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 82.50 Dissolved Date/Time Gallons Purged (gal) Conductivity (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 5/16/2022 12:17 64.44 3727 6.54 15.31 265 43.2 15.9 5/16/2022 12:18 64.66 3725 6.56 15.30 265 43.3 15.7 5/16/2022 12:19 64.88 3727 6.54 15.31 265 43.2 15.9 5/16/2022 12:20 65.10 3727 6.54 15.31 264 43.3 15.9 Pumping Rate Calculations !volume of water purged (g~ls) 65.10 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 289.48 [ Final Depth to Water (feet) 87.55 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Sc1mples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number I Type Sample Filtered? Type I Added? Total Dissolved Soilds y WATER 1 1 250-ml HOPE u 4 Deg C I y Comments: [ Ar~ved on site at 0715. Purge ~egan at 0720. Purged well for a total of 300 minutes. Purge ended and samples collected at 1220. Water was clear. Left site at 1228. Signature of Field Technician ~«.i'~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan SF-:_,-.· :,--_. 1· :r . ,, J' ----t _ /_· '_-_ -~·r ~ __ r ~YFP:e:Y s White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-35 Sampling Program Sampling Program Field Sample ID MW-35 04122022 Sampling Event Sampling Event 2022 Q2 GW Quarterly 2022 Q2 GW Quarterly Purge Date & Time 4/12/2022 13:02 Sample Date & Time 4/12/2022 14:20 !sampler lsallle_ler I TH/DL TH/DL I Purging Equipment Pump Weather Conditions Cloudy Pump Type QED External Ambient Temperature (C) 5 Purging Method 2 Casings Previous Well Sampled MW-02 Casing Volume (gal) 8.14 Calculated Casing Volumes Purge Duration (min) 75.11 pH Buffer 7.0 7.0 Well Depth (ft) 124.50 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 112.02 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/12/2022 14:17 16.70 4084 6.70 14.38 309 0 0 4/12/2022 14:18 16.92 4079 6.71 14.50 307 0 0 4/12/2022 14:19 17.14 4059 6.71 14.40 306 0 0 4/12/2022 14:20 17.36 4070 6.71 14.42 305 0 0 !volume of water purged (gals) Pumping Rate Calculations 17.36 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 80.00 [Final Depth to Water (feet) 112.93 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: I Arrived on site at 1257_ Purge beg_an at 1300. P_LJ_rged well for a total of 80_ minutes. Purge ended and samples collected at 1420. Water was clear. Left site at 1430. Signature of Field Technician ~ ..... ~,' ~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-36 Sampling_ Program Field Sample ID MW-36_04212022 Sampling_ Event 2022 Q2 GW Quarterly Purge Date & Time 4/21/2022 6:30 Sample Date & Time 4/21/2022 7:40 [sampler TH/DL Purgin_g Eguipment Pump Weather Conditions Clear Pump Type QED External Ambient Temperature (C) 8 Purging Method 2 Casings Previous Well Sampled MW-26 Casing Volume (gal) 7.26 Calculated Casing_ yolumes Purge Duration (min) 66.98 pH Buffer 7.0 7.0 Well Depth (ft) 121.60 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 110.47 Conductivity Dissolved Date/Time Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/21/2022 7:37 14.53 4812 7.03 14.40 279 0 73.0 4/21/2022 7:38 14.75 4833 7.02 14.45 278 0 71.0 4/21/2022 7:39 14.97 4820 7.02 14.35 278 0 71.4 4/21/2022 7:40 15.19 4824 7.02 14.30 278 0 71.6 Pumping Rate Calculations [volume of water purged (g_!ls) 15.19 Flow Rate (Q = S/60} (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 70.00 [ Final Depth to Water (feet) 111.08 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2504 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: I Arrived on site at 0626. Purge began at 0630. Pu rged well for a total of 70 minutes. Purge ended and samples collected at 0740. Water was clear. Left site at 0757. Signature of Field Technician ~=~-1-A~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-37 Sampling Program Field Sample ID MW-37 05172022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/26/2022 0:00 Sample Date & Time 5/17/2022 8:30 I sampler I TH/DL Purging Equipment Bailer Weather Conditions Cloudy Pump Type External Ambient Temperature (C) 18 Purging Method 2 Casings Previous Well Sampled MW-20 Casing Volume (gal) 10.39 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 121.80 pH Buffer 4.0 4.0 Well Casing Diameter O 4 Specific Conductance () 1000 Depth to Water Before Purging (ft) 105.88 Conductivity Dissolved Date/Time Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 5/4/2022 13:19 6.00 4332 6.54 14.23 290 36.7 68.0 5/17/2022 8:30 4458 7.08 14.86 Before 5/17/2022 8:36 4467 7.04 14.80 After [volume of water purged (gal) Pumping_ Rate Calculations 14.50 - Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () [Final Depth to Water (feet) 121.45 Number of casing Volumes 1.39 Volume, if well evacuated to dryness () 14.50 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds V WATER 1 250-ml HOPE u 4 Deg C V Heavy Metals -Full Suite V WATER 1 250-ml HOPE V HN03 (pH<2) V VOCs -Full Suite for GW V WATER 3 40mlVOA u HCI (pH<2), 4 Deg C V Nutrients V WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C V General lnorganics V WATER 1 250-ml HDPE u 4 Deg C V Gross Alpha V WATER 1 250-ml HOPE V HN03 V Comments: Arrived on site at 1309. Bailing began at 1314. Bailed a total of 14.50 gallons of water from the well. Purged well dry. Bailing ended at 1337. Water was a little murky. Left site at 1339.Arrived on site at 0827. Depth to water was 112.93. Samples bailed and collected at 0830. Left site at 0839. Signature of Field Technician ~u_,~+Ad~ I Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-38 Sampling Program Field Sample ID MW-38 04272022 Sampling_ Event 2022 Q2 GW Quarterly Purge Date & Time 4/26/2022 12:44 Sample Date & Time 4/27/2022 10:30 !sampler TH/DL Purging Equipment Bailer Weather Conditions Cloudy Pump Type Grundfos External Ambient Temperature (C) 19 Purging Method 2 Casings Previous Well Sampled MW-20 Casing Volume (gal) 2.77 Calculated Casing Volumes Purge Duration () pH Buffer 7 .0 7.0 Well Depth (ft) 74.40 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 70.15 Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/26/2022 12:52 5.00 4297 5.80 15.84 515 132.0 90.8 4/27/2022 10:30 4271 7.12 15.68 Before 4/27/2022 10:35 4262 7.13 15.60 After Pumping Rate Calculations !volume of water purged (gals} 5.00 Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () jFinal Depth to Water (feet) 74.37 Number of casing Volumes 1.80 Volume, if well evacuated to dryness (gals) 5.00 Name of Certified Analytical Laboratory AWSL Anal~i~I Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-mL HDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-mL HDPE u 4 Deg C y Gross Alpha y WATER 1 250-mL HDPE y HN03 y Comments: Arrived on site at 1244. Bailing began at 1247. Bailed a total of 5 gallons from well. Bailed well dry. Water was murky. Bailing ended at 1256. Left site at 1258. Arrived on site at 1025. Depth to water was 70.16. Samp_les bailed and collected at 1030. Left site at 1037. Signature of Field Technician --=3~~-h Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan S -~~1,-.-/ r -... · "•' " .-~ ,-~ 'E7VERGY~ ' --~" ~ .,. White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-39 Sampling Program Field Sample ID MW-39 04202022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/20/2022 7:00 Sample Date & Time 4/20/2022 11:00 !sampler I TH/DL I Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 9 Purging Method 2 Casings Previous Well Sampled MW-28 Casing Volume (gal) 24.95 Calculated Casing Volumes Purge Duration (min) 230.02 pH Buffer 7.0 7.0 Well Depth (ft) 102.50 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 64.28 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units} Temp (deg C) Redox (mV) Turbidity (NTU} Oxygen(%) Before/ After 4/20/2022 10:57 51.42 4706 4.02 15.20 531 2.7 0 4/20/2022 10:58 51.64 4691 4.00 15.04 540 2.8 0 4/20/2022 10:59 51.86 4693 4.00 15.07 539 2.8 0 4/20/2022 11:00 52.08 4697 4.00 15.01 539 2.9 0 [volum~ of wate! purged (gals) 52.08 Pumeing Rate Calculations Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 240.00 jFinal Depth to Water (feet) 68.40 Number of casing Volumes 2.00 Volume, if well evacuated to dryness() 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: [ Arrived on site at 0656. P_LJrg13_ began at 0700. Pu rged well for a totcll_ of 240 minutes. Purge ended and samples collected at 1100. Left site at 1109. Water was clear. Signature of Field Technician ~~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-40 Sampling Program Field Sample ID MW-40 04192022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/19/2022 9:45 Sample Date & Time 4/19/2022 13:50 !sampler I TH/DL I Purging Equipment Pump Weather Conditions Cloudy and windy Pump Type QED External Ambient Temperature (C) 15 Purging Method 2 Casings Previous Well Sampled MW-15 Casing Volume (gal) 26.39 Calculated Casing Volumes Purge Duration (min) 243.26 pH Buffer 7.0 7.0 Well Depth (ft) 120.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 79.58 Conductivity Dissolved Date/Time Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4/19/2022 13:47 52.51 3951 6.86 15.40 320 2.0 111.0 4/19/2022 13:48 52.73 3888 6.81 15.65 320 2.8 109.0 4/19/2022 13:49 52.94 3895 6.77 15.50 320 2.5 109.2 4/19/2022 13:50 53.16 3901 6.76 15.39 321 2.4 109.1 Pumping Rate Calculations [volume of water purged (gals) 53.16 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 245.00 [ Final Depth to WatE!r (feet) 80.27 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: [ Arrived on site at 0942. Purge began at 0945. Purged well for a total of 245 minutes. Purge ended and samples collected at 1350. Water was clear. Left site at 1400. Signature of Field Technician Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID TW4-24 Sampling Program Field Sample ID TW4-24_04272022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time 4/27/2022 12:29 Sample Date & Time 4/27/2022 12:30 !Sampler TH/DL Purging Equipment Pump Weather Conditions Cloudy Pump Type Grundfos External Ambient Temperature (C) 20 Purging Method 2 Casings Previous Well Sampled MW-26 Casing Volume (gal) 30.86 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 114.80 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 67.54 Conductivity Dissolved Date/Time Gallons Purged (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 4/27/2022 12:30 11117 6.70 16.56 311 4.1 20.0 Pumping Rate Calculations !volume of water purged() Flow Rate (Q = S/60) (gal/min) 15.00 Time to evacuate 2 Casing Volumes () !Final Depth to Water (feet) 70.23 Number of casing Volumes Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory GEL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Gross Alpha y WATER 1 250-ml HOPE y HN03 y Total Dissolved Soilds y WATER 1 250-ml HOPE u 4DegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Comments: I Arrived on site at 1225. Samples collected at 1230. Water was clear. Left site at 1236. Signature of Field Technician -2>~-M- Groundwater Discharge Permit ew;:-:/ r--, 1.· ;,-~. :-i, ~ .. I'~· l ~y~ -.? .-,• White Mesa Mill Field Data Worksheet For Groundwater Groundwater Monitoring Quality Assurance Plan Location ID MW-65 Sampling Program Field Sample ID MW-65_04142022 Sampling Event 2022 Q2 GW Quarterly Purge Date & Time Sample Date & Time 4/14/2022 10:05 !Sampler TH/DL Purging Equipment Weather Conditions Pump Type External Ambient Temperature () Purging Method Previous Well Sampled Casing Volume () Calculated Casing Volumes Purge Duration O pH Buffer 7 .0 Well Depth (ft) pH Buffer 4.0 Well Casing Diameter () Specific Conductance () Depth to Water Before Purging (ft) Date/Time Gallons Purged Conductivity pH Temp Redox Turbidity Dissolved Oxygen I Before/After J Pumping Rate Calculations !Volume of water purged() Flow Rate .{Q = S/60) () !Final Depth to Water (feet) Time to evacuate 2 Casing Volumes () Number of casing Volumes Volume, if well evacuated to dryness () Name of Certified Analytical Labor_atoiy AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soi Ids y WATER 1 250-ml HOPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250°ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 DegC y Gross Alpha y WATER 1 250-ml HOPE u HN03 y Comments: [ Du_plicate of MW-29 Signature of Field Technician ~~~H~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-70 Sampling Program Field Sample ID MW-70 04212022 Samplin_g Event 2022 Q2 GW Quarterly Purge Date & Time Sample Date & Time 4/21/2022 7:40 !sampler TH/DL Purging Equipment Weather Conditions Pump Type External Ambient Temperature () Purging Method Previous Well Sampled Casing Volume() Calculated Casing Volumes Purge Duration () pH Buffer 7 .0 Well Depth (ft) pH Buffer 4.0 Well Casing Diameter O Specific Conductance () Depth to Water Before Purging (ft) Date!Time Gallons Purged Conductivity pH Temp Redox Turbidity Dissolved Oxygen I Before/ After ] Pumping Rate Calculations !volume of water purged Q Flow Rate _{Q = S/60) () Time to evacuate 2 Casing Volumes () I Final Depth to Water (feet) Number of casing_ Volumes Volume, if well evacuated to dryness () Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: I Duplicate of MW-36 Signature of Field Technician TabC Field Data Worksheets Accelerated Monitoring Tab Cl Field Data Worksheets Accelerated Monitoring May 2022 Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-11 Sampling Program Field Sample ID MW-11 05042022 Sampling Event May Monthly Purge Date & Time 5/4/2022 7:05 Sample Date & Time 5/4/2022 11:40 !sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 4 Purging Method 2 Casings Previous Well Sampled MW-30 Casing Volume (gal) 29.31 Calculated Casing Volumes Purge Duration (min) 270.22 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 85.10 Conductivity Dissolved Date/Time Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 5/4/2022 11:37 59.02 3093 7.40 14.60 326 0 0 5/4/2022 11:38 59.24 3090 7.40 14.55 325 0 1.0 5/4/2022 11:39 59.45 3083 7.40 14.50 324 0 1.1 5/4/2022 11:40 59.67 3076 7.39 14.51 324 0 1.1 !volume of water purged (gals} 59.67 Pumping_ Rate Calculations Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 275.00 !Final Depth to Water (fee_t) 85.36 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-mL Poly u None N Heavy Metals -Mn only y WATER 1 250-ml HOPE y HN03 (pH<2) y Sulfate y WATER 1 250-ml HOPE u None N Total Dissolved Soi Ids y WATER 1 250-ml HOPE u 4 Deg C y Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y Comments: I Arrived _on site at 0700. Purge began at 0705. Purged well for a total of 275 minutes. Purge ended and s~ples collected at 1140. Water was clear. Left site at 1146. Signature of Field Technician ~=~~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-25 Sampling Program Sameling Program Field Sample ID MW-25 05032022 Sampling Event Sampling Event May Monthly May Monthly Purge Date & Time 5/3/2022 8:55 Sample Date & Time 5/3/2022 12:25 !sampler !sampler I TH/DL TH/DL Purging Equipment Pump Weather Conditions Cloudy and windy Pump Type QED External Ambient Temperature (C) 15 Purging Method 2 Casings Previous Well Sampled MW-31 Casing Volume (gal) 21.92 Calculated Casing Volumes Purge Duration (min) 202.03 pH Buffer 7.0 7.0 Well Depth (ft) 115.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 81.43 Conductivity Dissolved Date/Time Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 5/3/2022 12:22 44.91 3119 6.90 15.10 324 70.1 4.3 5/3/2022 12:23 45.13 3130 6.88 15.06 324 72.0 5.0 5/3/2022 12:24 45.35 3110 6.84 15.09 324 75.0 4.9 5/3/2022 12:25 45.57 3115 6.84 15.04 324 75.0 4.8 Pumping Rate Calculations [volume of water purged (gals) 45.57 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 §nal Depth to Water (feet) 83.35 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analyt~cal Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number I Type Sample Filtered? Type I Added? Total Dissolved Soilds y WATER 1 I 250-ml HOPE u 4 Deg C I y Comments: Arrived on site at 0851 . Purge began at 0855. Purged well for a total of 210 minutes. Purge ended and samples collected at 1225. Water was clear but had tiny little bubbles surfacing. Left site at 1228. Signature of Field Technician I Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan e . .._. 'F-:·. .... ·· /~ .' l," y ~· .__-: / C .--;-· ~Yl"VELS -~!___ . .r White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-26 Sampling Program Field Sample ID MW-26 05042022 Sampling Event May Monthly Purge Date & Time 5/4/2022 12:44 Sample Date & Time 5/4/2022 12:45 [sam_eler TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type Grundfos External Ambient Temperature (C) 11 Purging Method 2 Casings Previous Well Sampled MW-11 Casing Volume (gal) 28.92 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 121.33 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 77.04 Conductivity Dissolved Date/Time Gallons Purged (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 5/4/2022 12:45 3548 6.90 15.80 296 0 33.5 Pumping Rate Calculations [volume of water purged () Flow Rate {Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes () !Final Depth to Water (feet) 89.39 Number of casing Volumes Volume, if well evacuated to dryness () 0 Name of Certified Analytic_al Laboratory_ AWSL Analyt_ical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y voes-Chloroform y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Comments: I Arrived on site at 1240. Samples collected at 1245. Water was clear. Left site at 1250. Signature of Field Technician ~=~ ~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-30 Sampling Program Field Sample ID MW-30 05042022 Sampl_i_rlg_ Event May Monthly Purge Date & Time 5/4/2022 6:55 Sample Date & Time 5/4/2022 10:25 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 4 Purging Method 2 Casings Previous Well Sampled MW-25 Casin_g_ Volume (gal) 22.78 Calculated Casing Volumes Purge Duration (min) 209.98 _..., ........ "' pH Buffer 7.0 7.0 Well Depth (ft) 110.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 75.11 Conductivity Dissolved DatefTime Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 5/4/2022 10:22 44.91 2200 7.32 15.00 312 0 54.2 5/4/2022 10:23 45.13 2197 7.28 14.92 311 0 53.6 5/4/2022 10:24 44.35 2197 7.26 14.90 311 0 53.5 5/4/2022 10:25 45.57 2197 7.24 14.87 311 0 53.4 Pumping Rate Calculations [volume of water purged (gal~1 45.57 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 [Final Depth to Water (feet) 77.65 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y Heavy Metals -U and Se only y WATER 1 250-ml HOPE y HN03 (pH<2) y Total Dissolved Soi Ids y WATER 1 250-ml HOPE u 4 Deg C y Comments: [ Arrived on site at 0650. Purge began at 0655. Purged well for a total of 210 minutes. Purge ended and samples collected at 1025. Water was clear. Left site at 1035. Signature of Field Technician ~u.r-.,v__,;c__, Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-31 Sampling Program Sampling_!>!ogram Field Sample ID MW-31 05032022 Sampling Event Sameling Event May Monthly May Monthly Purge Date & Time 5/3/2022 8:45 Sample Date & Time 5/3/2022 14:55 !sampler [sampler I TH/DL TH/DL I Purging Equipment Pump Weather Conditions Cloudy and windy Pump Type QED External Ambient Temperature (C} 15 Purging Method 2 Casings Previous Well Sampled N/A Casing Volume (gal) 39.70 Calculated Casing Volumes Purge Duration (min) 365.92 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 69.20 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 5/3/2022 14:52 79.63 3323 7.00 15.00 320 10.0 111.0 5/3/2022 14:53 79.85 3318 7.05 14.87 319 10.0 111.0 5/3/2022 14:54 80.07 3328 7.10 14.85 319 11.0 110.9 5/3/2022 14:55 80.29 3325 7.10 14.86 319 11.0 110.9 [volume of water purged (gals) 80.29 Pumping_ Rate Calculations Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 370.00 [Fina_l___!)e_eth to Water (feet) 74.21 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HDPE u H2504 (pH<2), 4 Deg C y Sulfate y WATER 1 250-ml HDPE u None N Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 DegC y Heavy Metals -U only y WATER 1 250-ml HDPE y HN03 (pH<2) y Comments: I Arrived on site at 0840. P_uril~_beg_an at 0845. Purged well for a total of 370 minutes. Purge ended and samples collected at 1455. Water was mostly clear. Left site at 1503. Signature of Field Technician -:3~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-65 Sampling Program Field Sample ID MW-65 05042022 Sampling_ Event May Monthly Purge Date & Time Sample Date & Time 5/4/2022 10:25 [sampler TH/DL Purging Equipment Weather Conditions Pump Type External Ambient Temperature O Purging Method Previous Well Sampled Casing Volume O Calculated Casing Volumes Purge Duration O pH Buffer 7.0 Well Depth (ft) pH Buffer 4.0 Well Casing Diameter () Specific Conductance () Depth to Water Before Purging (ft) Date!Time Gallons Purg_ed Conductivity_ pH Temp Redox Turbidity Dissolved Oxygen I Before/ After ] Pumping Rate Calculations !Volume of water purged O Flow Rate (Q = S/60) ()_ Time to evacuate 2 Casing_ Volumes () !Final Depth to Water (feet) Number of casing Volumes Volume, if well evacuated to dryness () Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y Heavy Metals -U and Se only y WATER 1 250-ml HOPE y HN03 (pH<2) y Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Comments: Due_licate of MW-30 Signature of Field Technician ~CLJV1£~~ TabC2 Field Data Worksheets Accelerated Monitoring June 2022 Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan e -~I --' .. r"r . : ;, ~-------F?:e=Z s ---:-k"I. I ~-I .·._' White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-11 Sampling Program Field Sample ID MW-11 06062022 Samplin_g Event June Monthly Purge Date & Time 6/6/2022 7:45 Sample Date & Time 6/6/2022 12:20 !sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 23 Purging Method 2 Casings Previous Well Sampled MW-31 Casing Volume (gal) 29.36 Calculated Casing Volumes Purge Duration (min) 270.64 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 85.03 Conductivity Dissolved DatefTime Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 6/6/2022 12:17 59.02 3074 7.54 15.40 449 125.0 3.0 6/6/2022 12:18 59.24 3082 7.52 15.37 439 130.0 3.0 6/6/2022 12:19 59.45 3056 7.50 15.38 433 132.0 2.9 6/6/2022 12:20 59.67 3067 7.50 15.40 427 134.0 2.9 Pumping Rate Calculations - [volume of water purged (gals) 59.67 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 275.00 [ Final Depth to Water (feet) 86.39 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Heavy Metals -Mn only y WATER 1 250-ml HDPE y HN03 (pH<2) y Sulfate y WATER 1 250-ml HDPE u None N Total Dissolved Soilds y WATER 1 250-ml HDPE u 4DegC y Nitrate/nitrite as N y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y Comments: i Arrived on site at 07 40. Purge began at 07 45. Purged well for a total of 275 minutes. Purge ended and samples collected at 1220. Water was clear and had _ti_rly little bubbles surfacing_. Signature of Field Technician ~...r~~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-25 Sampling P!ogram Field Sample ID MW-25 06072022 Sampling Event June Monthly Purge Date & Time 6/7/2022 7:05 Sample Date & Time 6/7/2022 10:35 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 23 Purging Method 2 Casings Previous Well Sampled MW-30 Casing Volume (gal) 21.77 Calculated Casing Volumes Purge Duration (min) 200.65 pH Buffer 7.0 7.0 Well Depth (ft) 115.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 81.66 Conductivity Dissolved Date/Time Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 6/7/2022 10:32 44.91 3173 6.95 15.87 467 0 51.0 6/7/2022 10:33 45.13 3149 6.91 15.85 471 1.0 50.0 6/7/2022 10:34 45.35 3181 6.90 15.69 475 1.0 52.0 6/7/2022 10:35 45.57 3176 6.88 15.60 477 1.0 51.0 Pumping Rate Calculations - btolume of water purged (gals) 45 .57 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 [ Final Depth to Water (feet) 83.58 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number I Type Sample Filtered? Type I Added? Total Dissolved Soilds y WATER 1 I 250-ml HOPE u 4 Deg C I y Comments: [ Arrived on site at 0701 . Purge began at 0705. Purged well for a total o!J10 rriir11Jtes. Purge ended and samples collected at 1035. Water was clear. Left site at 1040. Signature of Field Technician ~~ ~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-26 Sampling Prog_ram Field Sample ID MW-26 06072022 Sampling Event June Monthly_ Purge Date & Time 6/7/2022 12:30 Sample Date & Time 6/7/2022 12:30 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type Grundfos External Ambient Temperature (C) 31 Purging Method 2 Casings Previous Well Sampled MW-25 Casing Volume (gal) 28.72 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 121.33 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 77.34 Conductivity Dissolved Date/Time Gallons Purged (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 6/7/2022 12:30 3404 6.84 18.01 277 0 29.0 Pumping Rate Calculations [volume of water purged() Flow Rate (Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes () [Final De_pth to Water (feet) 98.47 Number of casin_g Volumes Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytica_l_5amples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-mL Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y voes-Chloroform y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Comments: I Arrived on_ site at 1225. ~_mples collected at 1230. Water was clear. Left site at 1234. Signature of Field Technician ~=~-./-/.;, Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-30 Sampling Program Field Sample ID MW-30 06072022 Sampling Event June Monthly Purge Date & Time 6/7/2022 6:50 Sample Date & Time 6/7/2022 10:25 !sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 21 Purging Method 2 Casings Previous Well Sampled MW-11 Casing Volume (gal) 22.81 Calculated Casing Volumes Purge Duration (min) 210.28 pH Buffer 7.0 7.0 Well Depth (ft) 110.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 75.06 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 6/7/2022 10:22 46.00 2281 7.44 15.30 468 0 56.0 6/7/2022 10:23 46.22 2265 7.40 15.17 472 0 53.0 6/7/2022 10:24 46.43 2244 7.35 15.20 476 0 52.6 6/7/2022 10:25 46.65 2230 7.32 15.15 478 0 52.5 Pumping Rate Calculations [volume of water purged (gals) 46.65 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 215.00 [ Final Depth to Water (feet) 77.65 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y Heavy Metals -U and Se only y WATER 1 250-ml HDPE y HN03 (pH<2) y Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Comments: [ Arrived on site at 0646. P_ur_g_e began at 0650. Purged well for a total o_!_?15 minutes. Purge ended and samples collected at 1025. Water was clear. Left site at 1031 . Signature of Field Technician ~~r/"&-~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-31 Sampling Program Field Sample ID MW-31 06062022 Sampling Event June Monthly Purge Date & Time 6/6/2022 7:20 Sample Date & Time 6/6/2022 13:30 !sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C} 23 Purging Method 2 Casings Previous Well Sampled N/A Casing Volume (gal} 39.61 Calculated Casing Volumes Purge Duration (min} 365.07 pH Buffer 7.0 7.0 Well Depth (ft} 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 69.34 Conductivity Dissolved Date/Time Gallons Purged (gal} (um hos/cm) pH (pH Units) Temp (deg C} Redox (mV} Turbidity (NTU) Oxygen (%} Before/ After 6/6/2022 13:27 79.63 3407 7.28 15.51 459 1.2 114.0 6/6/2022 13:28 79.85 3403 7.18 15.50 463 1.0 115.0 6/6/2022 13:29 80.07 3434 7.16 15.45 465 1.1 114.0 6/6/2022 13:30 80.29 3424 7.13 15.48 465 1.0 114.0 Pumping Rate Calculations [volume _c:>f water purged (gals) 80.29 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 370.00 !Final C>eeth to Water (feet) 74.78 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y Sulfate y WATER 1 250-ml HDPE u None N Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -U only y WATER 1 250-ml HDPE y HN03 (pH<2) y Comments: I Arrived on site at 0715. Purge began at 0720. Pur_ged well for a total of 370 minutes. Purge ended and samples collected at 1330. Water was clear. Left site at 1338. Signature of Field Technician ~ ........ ~ Groundwater Discharge Permit SWf:. , .---: ' ,. -...___,· f ,_· ~-.. r ·.. .~. ,, ~YF:<."3CS -;,, ..I,! White Mesa Mill Field Data Worksheet For Groundwater Groundwater Monitoring Quality Assurance Plan Location ID MW-65 Sampling Program Field Sample ID MW-65 06072022 Sampling Event June Monthly Purge Date & Time Sample Date & Time 6/7/2022 10:35 !sampler TH/DL Purging Equipment Weather Conditions Pump Type . External Ambient Temperature() Purging Method Previous Well Sampled Casing Volume () Calculated Casing Volumes Purge Duration () pH Buffer 7.0 Well Depth (ft) pH Buffer 4.0 Well Casing Diameter () Specific Conductance () Depth to ~ater Before Purging (ft) Date/Time Gallons Purged Conductivity eH Temp Redox I Turbidity I Dissolved Oxygen I Before/After I Pumping_ Rate Calculations !Volume of water purged() Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes() [ Final Depth to Water (feet) Number of casing Volumes Volume, if well evacuated to dryness () Name of Certified Analytical Laboratory AWSL Analytical Sample.s Information Container Preservative Type of Sample/Analysis Sample Collected? Matrix Number I Type Sample Filtered? Type I Added? Total Dissolved Soilds y WATER 1 I 250-ml HDPE u 4 Deg C j y Comments: Duplicate of MW-25 Signature of Field Technician .2)=,.,.~~ TabD Quarter! y Depth to Water Name: Tanner Holliday, Deen Lyman 6/27 /2022-6/2 8/2022 Depth to Depth to Date Time Well Water (ft.) Date Time Well Water (ft.) 6/27/2022 1314 MW-01 65.08 6/28/2022 850 MW-04 81.95 6/27/2022 810 MW-02 109-65 6/28/2022 854 TW4-0I 105.23 6/27/2022 1039 MW-03A 84.08 6/28/2022 846 TW4-02 110.18 6/27/2022 1254 MW-05 108.28 6/28/2022 928 TW4-03 64.66 6/27/2022 1409 MW-II 85.29 6/28/2022 902 TW4-04 84.12 6/27/2022 1249 MW-12 109.68 6/28/2022 924 TW4-05 71.97 6/27/2022 1440 MW-14 102.02 6/28/2022 944 TW4-06 79.13 6/27/2022 1435 MW-15 105.46 6/28/2022 941 TW4-07 82.21 6/27/2022 1031 MW-17 72.09 6/28/2022 937 TW4-08 86.60 6/27/2022 1312 MW-18 74.25 6/28/2022 920 TW4-09 69.91 6/27/2022 1259 MW-19 66,67 6/28/2022 917 TW4-IO 69.42 6/27/2022 940 MW-20 88.01 6/28/2022 842 TW4-II 89.54 6/27/2022 923 MW-22 66.41 6/28/2022 1030 TW4-12 55.78 6/27/2022 1245 MW-23 113.97 6/28/2022 1026 TW4-13 56.83 6/27/2022 1239 MW-24A 110.65 6/28/2022 1018 TW4-14 77.37 6/27/2022 1236 MW-24 109.72 6/28/2022 914 TW4-16 73,72 6/27/2022 1322 MW-25 82.03 6/28/2022 1220 TW4-18 73.94 6/27/2022 837 MW-26 83.22 6/28/2022 740 TW4-19 72.17 6/27/2022 1040 MW-27 58.76 6/28/2022 815 TW4-21 72.15 6/27/2022 1231 MW-28 74.75 6/28/2022 750 TW4-22 69.51 6/27/2022 1228 MW-29 107.25 6/28/2022 1051 TW4-23 75.64 6/27/2022 1300 MW-30 75.48 6/28/2022 825 TW4-24 69.61 6/27/2022 1307 MW-31 69.75 6/28/2022 819 TW4-25 70.04 6/27/2022 1314 MW-32 82.88 6/28/2022 948 TW4-26 73.95 6/27/2022 1414 MW-33 DRY 6/28/2022 958 TW4-27 79.09 6/27/2022 1424 MW-34 107.39 6/28/2022 1034 TW4-28 49.25 6/27/2022 1417 MW-35 112.51 6/28/2022 954 TW4-29 78.38 6/27/2022 1420 MW-36 110.58 6/28/2022 1006 TW4-30 75.04 6/27/2022 1430 MW-37 106.82 6/28/2022 1002 TW4-31 76.28 6/27/2022 927 MW-38 70.22 6/28/2022 1038 TW4-32 56.28 6/27/2022 931 MW-39 64.65 6/28/2022 1043 TW4-33 78.16 6/27/2022 1023 MW-40 79.98 6/28/2022 949 TW4-34 77.58 6/28/2022 1010 TW4-35 75.40 MW-26=TW4-15 6/28/2022 1022 TW4-36 58.13 MW-32=TW4-17 6/28/2022 829 TW4-37 72.44 Comments: 6/28/2022 932 TW4-38 60.01 6/28/2022 833 TW4-39 70.77 6/28/2022 906 TW4-40 73.19 6/28/2022 858 TW4-41 89.99 6/28/2022 1047 TW4-42 69.77 6/28/2022 1014 TW4-43 73 .61 Date Time 6/28/2022 1256 6/28/2022 1304 6/28/2022 1054 6/28/2022 1126 6/28/2022 1121 6/28/2022 1203 6/28/2022 1130 6/28/2022 1059 6/28/2022 1049 6/28/2022 1308 6/28/2022 1315 6/28/2022 1253 6/28/2022 1250 6/28/2022 1044 6/28/2022 1247 6/28/2022 1325 6/28/2022 1322 6/28/2022 1027 6/28/2022 1024 6/28/2022 805 6/28/2022 1019 6/28/2022 1015 6/28/2022 1013 6/28/2022 1108 6/28/2022 1049 6/28/2022 1045 6/28/2022 1009 6/28/2022 935 6/28/2022 1006 6/28/2022 953 6/28/2022 950 6/28/2022 944 6/28/2022 1001 6/28/2022 947 6/28/2022 958 Well PIEZ-01 PJEZ-02 PJEZ-03A PJEZ-04 P!EZ-05 TWN-01 TWN-02 TWN-03 TWN-04 TWN-06 TWN-07 TWN-14 TWN-16 TWN-18 TWN-19 TWN-20 TWN-21 DR-05 DR-06 DR-07 DR-08 DR-09 DR-10 DR-II DR-12 DR-13 DR-14 DR-15 DR-17 DR-19 DR-20 DR-21 DR-22 DR-23 DR-24 Depth to Water (ft.) 67.64 46.90 54.55 67.28 65.95 70.18 58.69 44.22 63.18 81.05 80.41 59.35 48.00 63.11 54.50 78.17 79.29 83.30 94.01 92.08 51.40 86.72 78.42 97.93 DRY 69.78 76.34 92.98 64.75 63.33 55.53 100.72 DRY 70.59 44.83 TabE Laboratory Analytical Reports -Quarterly Sampling Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA60~ATORIE5 Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-01_04142022 Matrix: Water Date Sampled: 4/14/22 9:45 C"alrulalions Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnorl,!anil- Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 19.0 -1.2 18.5 1.0 234 < 1.0 0.05 15.9 0.3 < 0.1 707 1280 1220 < 0.0050 < 0.0005 < 0.0005 148 < 0.0250 <0.010 < 0.0100 0.30 < 0.0010 56.8 0.200 <0.0005 < 0.0100 < 0.0200 6.1 < 0.0050 <0.010 145 <0.0005 <0.10 < 0.0150 < 0.01 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 5.0 0.1 0.1 5.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030E SM 1030E SM2340B SM2320B SM2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1197 Preparation Date/Time 5/5/22 5/5/22 5/5/22 5/5/22 4/16/22 4/16/22 5/5/22 4/19/22 5/4/22 4/21/22 4/18/22 4/19/22 5/5/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/25/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22D1197-09 Analysis Date/Time 5/24/22 5/24/22 5/24/22 5/24/22 4/16/22 4/16/22 5/5/22 4/19/22 5/4/22 4/21/22 4/19/22 4/19/22 5/24/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 Page 19 of 44 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA80RATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-01_04142022 (cont.) Matrix: Water Date Sampled: 4/14/22 9:45 \ktal, fl'OIII.) Uranium, Dissolved < 0.0003 \ olatill' (hl,!a1111· ( 0111p1111111I, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran 7.3 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40 @ 0.9 °C Date Reported: 6/2/2022 Amended Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22D1197 Preparation Date/Time 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 2201197-09 Analysis Date/Time 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 J-LOW J-LOW J-LOW Page 20 of44 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 13, 2022 Company : Address : Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: ---- Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill G W MW-01 04142022 576962009 Ground Water 14-APR-22 09:45 19-APR-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.240 The following Analytical Methods were performed: Method MDC 0.831 RL 1.00 Project: Client ID: DNMIOOJOO DNMIOOI Units PF~ Analyst Date Time Batch Method pCi/L JXC9 05/10/22 1736 2261341 ~-~--------~-Analyst Comments __ Surrogate/Tracer Recovery Barium Carrier Notes: Test GFPC, Total Alpha Radium, Liquid "As Received" Counting Uncertainty is calculated at the 68% confidence level (I-sigma). Result __ Nominal ~covery% ~~ptable Limits 109 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: OF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 21 of 25 SDG: 576962 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-02_04122022 Matrix: Water Date Sampled: 4/12/22 13:35 ( akulafiom Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnor~anil· Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 43 .9 -4.7 39.9 1.3 232 < 1.0 < 0.05 5.8 0.3 <0.1 1920 3800 2870 < 0.0050 < 0.0005 < 0.0005 283 < 0.0250 <0.010 <0.0100 < 0.03 < 0.0010 86.8 < 0.0100 < 0.0005 < 0.0100 < 0.0200 9.4 0.0120 <0.010 424 < 0.0005 <0.10 <0.0150 < 0.01 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 5.0 0.1 0.1 50.0 500 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM 1030E SM 1030 E SM 1030E SM 2340 B SM2320B SM2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540 C SM 2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1197 Preparation Date/Time 5/5/22 5/5/22 5/5/22 5/5/22 4/16/22 4/16/22 5/5/22 4/19/22 5/4/22 4/21/22 4/18/22 4/18/22 5/5/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/25/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22D1197-03 Analysis Date/Time 5/24/22 5/24/22 5/24/22 5/24/22 4/16/22 4/16/22 5/5/22 4/19/22 5/4/22 4/21/22 4/19/22 4/18/22 5/24/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 Page 7 of 44 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-02_04122022 (cont.) Matrix: Water Date Sampled: 4/12/22 13:35 \Jt'tal, (l"Oll(.) Uranium, Dissolved 0.0117 \ olatill· Oq,!an1r ( 01111111111111, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 6/2/2022 Amended Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting Limit 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 LO Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22D1197 Preparation Date/Time 4/26/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 Lab ID: 22D1197-03 Analysis Date/Time 4/26/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 J-LOW J-LOW J-LOW Page 8 of 44 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 13, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: ---Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-02 04122022 576962003 Ground Water 12-APR-22 13:35 19-APR-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.249 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Surrogate/Tracer Recov~ Test MDC 0.686 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIOOlOO DNMIOOl Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/10/22 1735 2261341 Analyst Comme=n=ts,,__ -------- Result Nominal Recovery% Acceptable Limits 109 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 15 of 25 SDG: 576962 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 lA60RATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-03A_04272022 Matrix: Water Date Sampled: 4/27/22 9:15 ( ail'ulatiom Anions, Total Cation/Anion Balance Cations, Total TDS Ratio ln,11·t?,t111ir Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 75.2 -16 54.1 1.1 328 < 1.0 < 0,05 57.3 <0.1 0.4 3280 5080 4640 < 0.0050 < 0.0005 0.0009 208 < 0.0250 <0.010 < 0.0100 <0.04 < 0.0010 130 0.0832 < 0.0005 < 0.0100 < 0.0200 12.0 0.0874 < 0.010 753 0.0004 <0.10 < 0.0150 0.02 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 50.0 0.1 0.1 50.0 20 5 0.0050 0.0005 0.0005 0.4 0.0250 0.010 0.0100 0.04 0.0010 0.4 0.0100 0.0005 0.0100 0.0200 1.0 0.0050 0.010 1.0 0.0002 0.10 0.0150 0.01 PO#: Receipt: 4/29/22 11 :00 @ 0.0 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030 E SM 1030E SM2340B SM 2320B SM2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D2139 Preparation Date/Time 5/27/22 5/27/22 5/27/22 5/27/22 5/3/22 5/3/22 5/11/22 5/7/22 5/4/22 4/29/22 5/24/22 5/2/22 5/27/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/2/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 Lab ID: 22D2139-02 Analysis Date/Time 5/27/22 5/27/22 5/27/22 6/1/22 5/3/22 5/3/22 5/12/22 5/8/22 5/4/22 4/30/22 5/24/22 5/2/22 6/1/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/11/22 5/10/22 5/10/22 5/10/22 5/4/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/11/22 , 5/10/22 5/10/22 5/10/22 5/10/22 Page 5 of 35 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Lld30R1\TOftlES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-03A_04272022 (cont.) Matrix: Water Date Sampled: 4/27/22 9:15 \kral, fl'11111.) Uranium, Dissolved 0.0190 \ olalih-Organll' ( om110u1HI, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/29/22 11 :00@ 0.0 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22D2139 Preparation Date/Time 5/10/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 Lab ID: 22D2139-02 Analysis Date/Time 5/10/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 A-01 Page 6 of 35 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 26, 2022 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW -------------------Client Sample ID: MW-03A 04272022 Sample ID: 578558002 Matrix: Ground Water Collect Date: 27-APR-22 09: 15 Receive Date: 03-MA Y-22 Collector: Client Parameter Qualifier Result Uncertainty MDC Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.288 0.917 The following Analytical Methods were performed: Method Descriptio=n---------~ EPA 903.0 Surrogate/Tracer Recovery Test Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMI00100 DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/24/22 1311 2268525 Anal st Comments Result Nominal Recovery% Acceptable Limits ---103 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 14 of 22 SDG: 578558 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA80RATORlfS Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-05_04182022 Matrix: Water Date Sampled: 4/18/22 15:00 C akulation, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnt•r!!anh.: Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 29.9 -1.5 29.0 1.0 292 < 1.0 0.2 49.5 0.8 0.3 1140 2080 1980 < 0.0050 < 0.0005 < 0.0005 119 < 0.0250 < 0.010 < 0.0100 < 0.03 < 0.0010 36.1 0.107 < 0.0005 < 0.0100 < 0.0200 7.0 < 0.0050 < 0.010 458 < 0.0005 < 0.10 < 0.0150 <0.01 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting !J..m..l! 1.0 1.0 0.05 1.0 0.1 0.1 20.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0,03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 2.5 0.0005 0.10 0.0150 O.ol PO#: Receipt: 4/22/22 13:30 @ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030 E SM 1030 E SM 23408 SM2320B SM 2320 B EPA350.l EPA300.0 EPA 300.0 EPA353.2 EPA 300.0 SM 2540C SM 2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA 200,8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1691 Preparation Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 4/27/22 4/27/22 4/25/22 4/27/22 4/25/22 5/17/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Lab ID: 2201691-01 Analysis Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 4/27/22 4/27/22 4/25/22 4/27/22 4/25/22 5/24/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/3/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Page 3 of 50 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 LABORATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-05_04182022 (cont.) Matrix: Water Date Sampled: 4/18/22 15:00 \ktals (l"OIII.) Uranium, Dissolved 0.0005 \ olalill· <>r-:!allll" ( 0111pou1ul, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < LO Chlorofonn < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting 1imi! 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22D1691 Preparation Date/Time 5/2/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 Lab ID: 2201691-01 Analysis Date/Time 5/2/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 A-OJ Page4 of50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 23, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW ------ Parameter Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW-05 _ 04182022 577764001 Ground Water 18-APR-22 15:00 26-APR-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.139 The following Analytical Methods were performed: Method Desc!iPtio~n ________ _ EPA 903.0 Surrogate/Tracer Recovery Test - MDC 0.585 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIOOIOO DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/18/22 1314 2265414 -~-AJ!a\yst Comments Result Nominal Recovery% Acceptable Limits 104 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 14 of 27 SDG: 577764 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 ll1BO~•HORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-11_04182022 Matrix: Water Date Sampled: 4/18/22 11:20 ( alnilation, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnort,!ani,: Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \leral, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 31.7 -5.9 28.2 1.0 267 < 1.0 0.4 54.9 0.3 2.2 1240 2060 2060 < 0.0050 < 0.0005 < 0.0005 106 < 0.0250 <0.010 < 0.0100 < 0.03 <0.0010 37.5 0.180 < 0.0005 < 0.0100 < 0.0200 7.0 0.0108 < 0.010 451 < 0.0005 < 0.10 < 0.0150 < 0.01 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 20.0 0.1 0.1 20.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030 E SM 1030E SM2340B SM 23208 SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1691 Preparation Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 4/27/22 5/2/22 4/25/22 4/27/22 4/25/22 5/17/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Lab ID: 22Dl691-02 Analysis Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 4/27/22 5/2/22 4/25/22 4/27/22 4/25/22 5/24/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/3/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Page 5 of 50 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD t A.90A~roa1c.1 Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-11_04182022 (cont.) Matrix: Water Date Sampled: 4/18/22 11:20 \lctals (rnnt.) Uranium, Dissolved 0.0019 \ olaltk Orl!anir ( ompoutHh Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A CtF WO#: 22D1691 Preparation Date/Time 5/2/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 Lab ID: 2201691-02 Analysis Date/Time 5/2/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 A-01 Page 6 of 50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 23, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-11 04182022 577764002 Ground Water 18-APR-22 11:20 26-APR-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.211 The following Analytical Methods were performed: Method__ Descri tion EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.712 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (}-sigma). RL 1.00 Project: Client ID: DNMI00100 DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/18/22 1314 2265414 Anal st Comments Result Nominal Recovery% Acceptable Limits 101 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 15 of27 SDG: 577764 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LASOR,\TOIIIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-12_04192022 Matrix: Water Date Sampled: 4/19/22 9:25 ( akulation~ Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Alkalinity· Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 52.7 -0.7 51.9 1.1 330 < 1.0 < 0.05 52.8 0.1 0.3 2200 3720 3400 < 0.0050 <0.0005 < 0.0005 443 < 0.0250 <0.010 < 0.0100 < 0.03 < 0.0010 209 0.0111 < 0.0005 < 0.0100 < 0.0200 12.5 0.0313 <0.010 282 < 0.0005 <0.10 < 0.0150 <0.01 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting !d.mi! 1.0 1.0 0.05 50.0 0.1 0.1 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030E SM 1030E SM 23408 SM2320B SM 23208 EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1691 Preparation Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 4/27/22 5/2/22 4/25/22 4/27/22 4/25/22 5/17/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Lab ID: 2201691-05 Analysis Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 4/27/22 5/2/22 4/25/22 4/27/22 4/25/22 5/24/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/3/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Page 11 of 50 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-12_04192022 (cont.) Matrix: Water Date Sampled: 4/19/22 9:25 \lctals (cont.) Uranium, Dissolved 0.0205 \ olatik OrganiL· ( 11111110111Hh Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chi oromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0025 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22D1691 Preparation Date/Time 5/2/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 Lab ID: 22D1691-05 Analysis Date/Time 5/2/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 A-01 Page 12 of 50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company : Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-12 04192022 577764005 Ground Water 19-APR-22 09:25 26-APR-22 Client Project: Client ID: Report Date: May 23, 2022 DNMIOOIOO DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method ----- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.154 0.517 1.00 pCi/L JXC9 05/18/22 1314 2265414 The following Analytical Methods were performed: -----------Method .Descri ti~ll---~ EPA 903.0 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 105 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level ( I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 18 of27 SDG: 577764 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l/~60R I\ TOR IE S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-14_04182022 Matrix: Water Date Sampled: 4/18/22 15:00 ( akulation, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio I nor~anit Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \lctal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 48.6 -2.9 45.9 I.I 345 < 1.0 <0.05 17.7 < 0.1 < 0.1 2040 3360 3130 < 0.0050 < 0.0005 0.0013 423 < 0.0250 <0.010 < 0.0100 < 0.03 < 0.0010 142 1.71 < 0.0005 <0.0100 <0.0200 I I.I <0.0050 <0.010 294 <0.0005 < 0.10 < 0.0150 0.01 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 1.0 0.1 0.1 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030 E SM 1030E SM2340B SM2320B SM2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540 C SM2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1691 Preparation Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 5/2/22 5/2/22 4/25/22 4/27/22 4/25/22 5/17/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Lab ID: 22D1691-03 Analysis Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 5/2/22 5/2/22 4/25/22 4/27/22 4/25/22 5/24/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/3/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Page 7 of 50 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-14_04182022 (cont.) Matrix: Water Date Sampled: 4/18/22 15:00 \lct:ils (cont.) Uranium, Dissolved 0.0610 \ olatik Ori:anll' ( ·ompouml, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22D1691 Preparation Date/Time 5/17/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 Lab ID: 2201691-03 Analysis Date/Time 5/17/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 A-01 Page 8 of 50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 23, 2022 Company: Address : Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW --- Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW-14 04182022 577764003 Ground Water 18-APR-22 15:00 26-APR-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.126 The following Analytical Methods were performed: Method Description _ EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.568 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMI00100 DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/18/22 1314 2265414 Anal st Comments Result Nominal Recovery% Acceptable Limits 106 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 16 of 27 SDG: 577764 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-15_04192022 Matrix: Water Date Sampled: 4/19/22 10:45 ("akulation, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio I nor:,!anit Alkalinity-Bicarbonate (as CaC03) Alkalinity-Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktab Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 50.7 -7.0 44.1 1.1 339 < 1.0 <0.05 36.0 0.2 0.2 2120 3460 3210 < 0.0050 < 0.0005 < 0.0005 336 < 0.0250 < 0.010 < 0.0100 <0.03 < 0.0010 134 < 0.0100 < 0.0005 < 0.0100 < 0.0200 8.6 0.120 <0.010 369 < 0.0005 < 0.10 < 0.0150 < o.oi Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 5.0 0.1 0.1 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030E SM 1030E SM2340B SM2320B SM2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1691 Preparation Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 5/2/22 5/2/22 4/25/22 4/27/22 4/25/22 5/17/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Lab ID: 22D1691-06 Analysis Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 5/2/22 5/2/22 4/25/22 4/27/22 4/25/22 5/24/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/3/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 A-Ola Page 13 of 50 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 Ll,8QAI\TOA1£S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-15_04192022 (cont.) Matrix: Water Date Sampled: 4/19/22 10:45 \lct:1h (rnnr.1 Uranium, Dissolved 0.0424 Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0025 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22D1691 Preparation Date/Time 5/2/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 Lab ID: 2201691-06 Analysis Date/Time 5/2/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 A-01 Page 14 of 50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 23, 2022 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-15 04192022 577764006 Ground Water l 9-APR-22 I 0:45 26-APR-22 Client Parameter ____ Qualifier Result Uncertain-'ty'--__ M_D_C_ Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.134 0.631 The following Analytical Methods were performed: ---------- RL 1.00 Project: Client ID: DNMIOOIOO DNMIOOI Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/18/22 1314 2265414 Method Description _______ A~na_lyst Comments EPA 903.0 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 101 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 19 of27 SDG: 577764 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA80RATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-17_04182022 Matrix: Water Date Sampled: 4/18/22 11:55 ( akulation, Anions, Total Cation/Anion Balance Cations, Total IDS Ratio lnor1!anil· Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (IDS) TDS, Calculated \l~1al, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Di~solved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 42.1 -1.4 41.0 1.0 333 < 1.0 < 0.05 31.5 0.2 1.1 1720 2820 2750 < 0.0050 < 0.0005 < 0.0005 245 < 0.0250 <0.010 < 0.0100 < O.o3 < 0.0010 130 0.0366 < 0.0005 < 0.0100 < 0.0200 9.3 0.0165 <0.010 410 < 0.0005 < 0.10 < 0.0150 < 0.01 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 1.0 0.1 0.1 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/22/22 13:30@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030 E SM 1030E SM2340 B SM2320B SM2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.J EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1691 Preparation Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 5/2/22 5/2/22 4/25/22 4/27/22 4/25/22 5/17/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Lab ID: 2201691-04 Analysis Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 5/2/22 5/2/22 4/25/22 4/27/22 4/25/22 5/24/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/3/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Page 9 of 50 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA80f;IATOfllfS Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-17 _04182022 (cont.) Matrix: Water Date Sampled: 4/18/22 11:55 \lctals (l'fllll.) Uranium, Dissolved 0.0372 \ olallll· On!llllll' < 11111pm11uh Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0050 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22D1691 Preparation Date/Time 5/2/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 Lab ID: 22D1691-04 Analysis Date/Time 5/2/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 A-01 Page 10 of 50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 23 , 2022 Company: Address : Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-17 04182022 577764004 Ground Water 18-APR-22 11 :55 26-APR-22 Client Parameter Qualifier Result Uncertainty MDC Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.182 0.538 The following Analytical Methods were performed: Project: Client ID: DNMIOOIOO DNMI001 RL Units PF DF Analyst Date Time Batch Method ---------- 1.00 pCi/L JXC9 05/18/22 1314 2265414 ---------------Method Descri tion -----------------Analyst Comm_e_nt_s __________ _ I EPA 903.0 Surrogate/Tracer Recovery Test __ _ Result Nominal ~overy% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 104 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: OF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 17 of 27 SDG: 577764 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l/d30RATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-18_04132022 Matrix: Water Date Sampled: 4/13/22 11:35 ( ak11lat1ons Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnor:.!ank Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 42.4 -0.7 41.8 1.6 278 < 1.0 <0.05 42.8 0.2 <0,1 1760 4400 2750 < 0.0050 < 0.0005 < 0.0005 486 < 0.0250 <0.010 < 0.0100 <0.03 < 0.0010 121 0.102 < 0.0005 < 0.0100 < 0.0200 7.2 < 0.0050 < 0.010 170 0.0022 < 0.10 < 0.0150 < 0.01 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 5.0 0.1 0.1 50.0 500 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM 1030£ SM 1030 E SM 1030 E SM2340B SM 23208 SM2320 B EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1197 Preparation Date/Time 5/5/22 5/5/22 5/5/22 5/5/22 4/16/22 4/16/22 5/5/22 4/19/22 5/4/22 4/21 /22 4/18/22 4/18/22 5/5/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/25/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22Dl197-07 Analysis Date/Time 5/24/22 5/24/22 5/24/22 5/24/22 4/16/22 4/16/22 5/5/22 4/19/22 5/4/22 4/21/22 4/19/22 4/18/22 5/24/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 Page 15 of 44 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-18_04132022 (cont.) Matrix: Water Date Sampled: 4/13/22 11:35 \lctals (rnnl.) Uranium, Dissolved 0,0265 \ olatill' Ori.:anir ( 01111111u1Hls Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofonn < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 6/2/2022 Amended Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting Limit 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 82600 /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22D1197 Preparation Date/Time 4/26/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 Lab ID: 22Dl197-07 Analysis Date/Time 4/26/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 J-LOW J-LOW J-LOW Page 16 of44 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-18 04132022 576962007 Ground Water 13-APR-22 11 :35 19-APR-22 Client --~--------- Project: Client ID: Report Date: May 13, 2022 DNMI00100 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.219 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Surrogate/Tracer Recovery T_e_st __ _ 0.637 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). --- 1.00 pCi/L JXC9 05/10/22 1736 2261341 Analyst Comments Result Nominal Recovery% Acceptable Limits 107 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: OF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 19 of 25 SDG: 576962 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit " I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABO~•\TORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-19_04132022 Matrix: Water Date Sampled: 4/13/22 13:35 ( alrulariun, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnor~anit. Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 13.8 0.2 13.8 3.2 135 < 1.0 <0.05 29.3 1.2 2.1 515 2900 886 < 0.0050 <0.0005 < 0.0005 119 < 0.0250 < 0.010 < 0.0100 <0.03 < 0.0010 46.0 < 0.0100 < 0.0005 < 0.0100 < 0.0200 4.2 0.0140 <0.010 91.5 < 0.0005 < 0.10 < 0.0150 <0.01 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting !dm.it 1.0 1.0 0.05 5.0 0.5 0.1 5.0 500 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM 1030E SM 1030 E SM 1030E SM2340B SM2320B SM2320B EPA350.1 EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1197 Preparation Date/Time 5/5/22 5/5/22 5/5/22 5/5/22 4/16/22 4/16/22 5/5/22 4/19/22 4/18/22 4/21/22 4/18/22 4/18/22 5/5/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/25/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22D1197-08 Analysis Date/Time 5/24/22 5/24/22 5/24/22 5/24/22 4/16/22 4/16/22 5/5/22 4/19/22 4/19/22 4/21/22 4/19/22 4/18/22 5/24/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 Page 17 of44 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LAllO~.ATORlfS Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-19_04132022 (cont.) Matrix: Water Date Sampled: 4/13/22 13:35 \I eta I, ( rnn I.) Uranium, Dissolved 0.0062 \ ol:ttik Oq:a111t· < 0111110u11th Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 6/2/2022 Amended Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting Limit 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22D1197 Preparation Date/Time 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22Dl197-08 Analysis Date/Time 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 J-LOW J-LOW J-LOW Page 18 of 44 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 13, 2022 Company : Address : Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-19 04132022 576962008 Ground Water 13-APR-22 13:35 19-APR-22 Client --- Qualifier Result Uncertainty ---- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.283 _The following Analytical Methods were perform_e_d_: __ Method __ Descdption EPA 903.0 Surrog~te/Tracer Recovery Test --- MDC 0.839 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: Units PF pCi/L DNMIOOIOO DNMIOOI OF Analyst Date Time Batch Method JXC9 05/10/22 1736 2261341 Analyst Commen=tsc.__ Result Nominal Recovery% Acceptable Limits 101 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 20 of25 SDG: 576962 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l A60R >\TO A IE S Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-20_05172022 Matrix: Water Date Sampled: 5/17/22 8:00 ( aln1lation, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio I norcanir Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \let iii, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 61.7 2.2 64.5 1.0 83.5 < 1.0 < 0.05 60.9 0.2 8.2 2820 4450 4350 < 0.0050 < 0.0005 < 0.0005 288 < 0.0250 <0.010 < 0.0100 < 0.10 < 0.0010 31.2 < 0.0100 < 0.0005 0.0144 < 0.0200 24.3 < 0.0050 < 0.010 1080 <0.0002 <0.10 < 0.0150 < 0.01 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 1.0 0.1 0.5 100 20 5 0.0050 0.0005 0.0005 1.0 0.0250 0.010 0.0100 0.10 0.0010 1.0 0.0100 0.0005 0.0100 0.0200 2.5 0.0050 0.010 2.5 0.0002 0.10 0.0150 0.01 PO#: Receipt: 5/18/22 12:20@ 0.8 °C Date Reported: 6/3/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM IOJOE SM 1030E SM IOJOE SM 23408 SM2320B SM2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22E 1503 Prep11ration Date/Time 6/2/22 6/2/22 6/2/22 6/2/22 5/24/22 5/24/22 5/27/22 5/25/22 5/25/22 5/24/22 5/31/22 5/19/22 6/2/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/18/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 Lab ID: 22E1503-01 Analysis Date/Time 6/2/22 6/2/22 6/2/22 6/2/22 5/24/22 5/24/22 5/27/22 5/25/22 5/25/22 5/24/22 5/31/22 5/19/22 6/2/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/20/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 Page 3 of 24 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA60R~TORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-20_05172022 (cont.) Matrix: Water Date Sampled: 5/17/22 8:00 \lrtal, (COIII.) Uranium, Dissolved 0.0021 \ olatik Ori,:anll' ( 01111H1111HI, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 5/18/22 12:20@ 0.8 ·c Date Reported: 6/3/2022 Amended Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22E1503 Preparation Date/Time 5/27/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 Lab ID: 22El503-01 Analysis Date/Time 5/27/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 J-LOW J-LOW Page 4 of24 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: June 16, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 . Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-20 05172022 580437001 Ground Water 17-MAY-22 08:00 19-MAY-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.160 The following Analytical Methods were performed: Method __ DescriJ:>tion EPA 903.0 Surro~ate/Tracer Recovery T_es_t __ _ MDC 0.558 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (]-sigma). RL 1.00 Project: Client ID: DNMIOOIOO DNMIOOI Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/24/22 1312 2268525 Anal st Comments __ _ Result Nominal Recovery% Acce_etable Limits 112 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 12 of 15 SDG: 580437 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD t~I 0 1tA.tOlt1ts Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-22_04252022 Matrix: Water Date Sampled: 4/25/22 12:50 ("ak11la1i11n, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnorcanir Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 127 -7.2 110 1.6 < 1.0 < 1.0 0.8 51.8 10.8 1.8 6040 12000 7680 < 0.0050 0.0117 0.155 328 < 0.0250 0.436 0.0937 0.12 0.0027 1010 50.9 < 0.0005 0.437 0.253 16.1 0.0393 <0.010 234 0.0020 < 0.10 < 0.0150 1.08 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 20.0 0.1 0.1 100 100 5 0.0050 0.0005 0.0005 1.0 0.0250 0.010 0.0100 0.10 0.0010 1.0 0.0250 0.0005 0.0100 0.0200 2.5 0.0050 0.010 2.5 0.0002 0.10 0.0150 0.01 PO#: Receipt: 4/29/22 11 :00 @ 0.0 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030 E SM 1030 E SM 2340 B SM2320B SM2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA 200.7 EPA200.8 EPA200.8 CtF WO#: 22D2139 Preparation Date/Time 5/27/22 5/27/22 5/27/22 5/27/22 5/3/22 5/3/22 5/11/22 5/7/22 5/4/22 4/29/22 5/7/22 5/2/22 5/27/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/2/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5110/22 5/10/22 5/10/22 5/10/22 Lab ID: 22D2139-01 Analysis Date/Time 5/27/22 5/27/22 5/27/22 6/1/22 5/3/22 5/3/22 5/12/22 5/8/22 5/4/22 4/30/22 5/8/22 5/2/22 6/1/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/11/22 5/10/22 5/11/22 5/10/22 5/4/22 5/10/22 5/10/22 5/11/22 5/10/22 5/10/22 5/11/22 5/10/22 5/11/22 5/10/22 5/10/22 Page 3 of 35 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA60R:,\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-22_04252022 (cont.) Matrix: Water Date Sampled: 4/25/22 12:50 \ lctal, ( run I.) Uranium, Dissolved 0.0205 \ ulatilt· Or).!an1t· ( 11111p11uml- Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/29/22 11 :00 @ o.o ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22D2139 Preparation Date/Time 5/10/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 Lab ID: 22D2139-01 Analysis Date/Time 5/10/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 A-01 Page 4 of 35 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: Project: ------ Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-22 042520222 578558001 Ground Water 25-APR-22 12:50 03-MAY-22 Client Project: Client ID: Report Date: May 26, 2022 DNMIOOIOO DNMIOOI Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 2.05 +/-0.439 0.724 1.00 pCi/L JXC9 05/24/22 13 l l 2268525 I he following Analytical Methods were performed: Method Descrip_ti_o_n __________________ _ EPA 903.0 Surrog~te/Tracer Recovery Test Result Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). Analy_st Comments Nominal Recovery% Acceptable Limits 96.6 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 13 of 22 SDG: 578558 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l1l.BOR1HORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-23_04272022 Matrix: Water Date Sampled: 4/27/22 8:40 ( alnilaliom Anions, Total Cation/Anion Balance Cations, Total TDS Ratio l norcanil- Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 52.0 -1.8 50.1 0.99 239 < 1.0 <0.05 7.7 0.2 0.1 2300 3370 3410 < 0.0050 < 0.0005 < 0.0005 426 < 0.0250 < 0.010 < 0.0100 < 0.03 < 0.0010 151 < 0.0100 < 0.0005 < 0.0100 < 0.0200 9.1 < 0.0050 <0.010 372 0.0003 < 0.10 < 0.0150 <0.01 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 1.0 0.1 0.1 100 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0002 0.10 0.0150 0.01 PO#: Receipt: 4/29/22 11 :OO @ o.o ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030 E SM 1030E SM2340B SM 2320B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D2139 Preparation Date/Time 5/27/22 5/27/22 5/27/22 5/27/22 5/3/22 5/3/22 5/11/22 5/8/22 5/4/22 4/29/22 5/7/22 5/2/22 5/27/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/2/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 Lab ID: 22D2139-03 Analysis Date/Time 5/27/22 5/27/22 5/27/22 6/1/22 5/3/22 5/3/22 5/12/22 5/9/22 5/4/22 4/30/22 5/8/22 5/2/22 6/1/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/4/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/11/22 5/10/22 5/10/22 5/10/22 5/10/22 Page 7 of 35 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/d30R:o\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-23_04272022 (cont.) Matrix: Water Date Sampled: 4/27/22 8:40 \lc1al, (rnnl.) Uranium, Dissolved 0.0100 \ olalik Ori:anll' < ompounll, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofonn < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/29/22 11 :00@ 0.0 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22D2139 Preparation Date/Time 5/10/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 Lab ID: 2202139-03 Analysis Date/Time 5/10/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 A-01 Page 8 of 35 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 26, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW ----- MW-23 04272022 578558003 Ground Water 27-APR-22 08:40 03-MAY-22 Client Qualifier Result Uncertainty ---Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.247 The following Analytical Methods were perfonned: Method Descri tion EPA903.0 Surroiate/Tracer Recovery Test MDC 0.689 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (]-sigma). RL 1.00 Project: Client ID: DNMIOOIOO DNMIOOl Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/24/22 1311 2268525 An!!lyst Comments Result Nominal Recovery% Acceptable Limits 112 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 15 of22 SDG: 578558 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 ll1BOR•\fORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-24_04272022 Matrix: Water Date Sampled: 4/27/22 8:00 ( aln,latiom Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnor:,!anit Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 66.1 -13 50.1 0.81 < 1.0 < 1.0 < 0.05 43.2 0.8 0.3 3120 3350 4120 < 0.0050 0.0025 0.0092 431 < 0.0250 0.119 0.0137 < 0.03 0.0022 162 7.07 < 0.0005 < 0.0100 0.0743 10.8 0.0152 < 0.010 355 0.0031 <0.10 < 0.0150 0.12 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 10.0 0.1 0.1 50.0 20 5 0.0050 0.0005 0.0005 1.0 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0002 0.10 0.0150 0.01 PO#: Receipt: 4/29/22 11 :00@ 0.0 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030E SM 1030 E SM 2340 B SM 2320 B SM23208 EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D2139 Preparation Date/Time 5/27/22 5/27/22 5/27/22 5/27/22 5/3/22 5/3/22 5/11/22 5/8/22 5/4/22 4/29/22 5/7/22 5/2/22 5/27/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/2/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 Lab ID: 2202139-04 Analysis Date/Time 5/27/22 5/27/22 5/27/22 6/1/22 5/3/22 5/3/22 5/12/22 5/9/22 5/4/22 4/30/22 5/8/22 5/2/22 6/1/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/11/22 5/10/22 5/11/22 5/10/22 5/4/22 5/10/22 5/10/22 5/11/22 5/10/22 5/10/22 5/11/22 5/10/22 5/10/22 5/10/22 5/10/22 Page 9 of 35 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA60RATOIIIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-24_04272022 (cont.) Matrix: Water Date Sampled: 4/27/22 8:00 \lctah (ront.) Uranium, Dissolved 0.0070 \ olatilt' Organir ( 0111p1111111l, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/29/22 11 :00 @ 0.0 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 82600 /5030A CtF WO#: 22D2139 Preparation Date/Time 5/10/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 Lab ID: 2202139-04 Analysis Date/Time 5/10/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 A-01 Page 10 of 35 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 26, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW ----------- Parameter Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW-24 04272022 578558004 Ground Water 27-APR-22 08:00 03-MAY-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 2.28 +/-0.432 The following Analytical Methods were performed: --~~ ---- MDC 0,666 RL 1.00 Project: Client ID: DNMI00100 DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/24/22 1311 2268525 Method _ Descri tion ---------------~Analyst Comments EPA 903.0 Surrogate/Tracer Recovery_ T_e_s_t __ Result Nominal Recovery% Acc~table Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 105 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 16 of 22 SDG: 578558 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-24A_04272022 Matrix: Water Date Sampled: 4127122 7:40 ( ah.:ulat10"' Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lno1·:.!.anil" Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktab Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 64.7 -16 47.1 0.95 < 1.0 < 1.0 0.07 43.3 1.2 0.2 3050 3800 3990 <0.0050 0.0043 0.0089 404 < 0.0250 0.121 0.0171 <0.03 < 0.0010 145 6.51 < 0.0005 < 0.0100 0.0604 9.6 0.0172 < 0.010 339 0.0027 < 0.10 < 0.0150 0.04 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 10.0 0.1 0.1 50.0 20 5 0.0050 0.0005 0.0005 1.0 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0002 0.10 0.0150 0.01 PO#: Receipt: 4/29/22 11 :oo@ o.o ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030 E SM 1030 E SM2340B SM 2320 B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D2139 Preparation Date/Time 5/27/22 5/27/22 5/27/22 5/27/22 5/3/22 5/3/22 5/11/22 5/8/22 5/4/22 4/29/22 5/7/22 5/2/22 5/27/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/2/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 Lab ID: 22D2139-05 Analysis Date/Time 5/27/22 5/27/22 5/27/22 6/1/22 5/4/22 5/4/22 5/12/22 5/9/22 5/4/22 4/30/22 5/8/22 5/2/22 6/1/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/11/22 5/10/22 5/11/22 5/10/22 5/4/22 5/10/22 5/10/22 5/11/22 5/10/22 5/10/22 5/11/22 5/10/22 5/10/22 5/10/22 5/10/22 Page 11 of 35 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA60~,'l,TORIE5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-24A_04272022 (cont.) Matrix: Water Date Sampled: 4/27/22 7:40 \lctals (rnnt.) Uranium, Dissolved 0.0086 \ olatill· Ori.:anir ( ompoumh Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/29/22 11 :00@ 0.0 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A CtF WO#: 22D2139 Preparation Date/Time 5/10/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 Lab ID: 22D2139-05 Analysis Date/Time 5/10/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 A-01 Page 12 of 35 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 26, 2022 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: ---Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-24A 04272022 578558005 Ground Water 27-APR-22 07:40 03-MAY-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 3.10 +/-0.493 The following Analytical Methods were performed: Method ---- Surrogate/Tracer Recovery Test MDC 0.563 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL Project: Client ID: DNMIOOIOO DNMIOOI Units PF DF Analyst Date Time Batch Method --- 1.00 pCi/L JXC9 05/24/22 1311 2268525 Analyst Comments Result Nominal Recovery% Acceptable Limits 106 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: OF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 17 of 22 SDG: 578558 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l/\80R,HOR1f5 Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-25_04122022 Matrix: Water Date Sampled: 4/12/22 10:55 ("akulalion, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia asN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 38.0 -3.1 35.8 1.5 246 < 1.0 0.4 33.4 0.3 <0.1 1590 3600 2450 < 0.0050 < 0.0005 0.0013 306 < 0.0250 <0.010 < 0.0100 < 0.03 < 0.0010 113 1.29 < 0.0005 0.0162 < 0.0200 8.8 < 0.0050 < 0.010 252 0.0009 < 0.10 < 0.0150 < 0.01 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.2 5.0 0.1 0.1 50.0 500 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030E SM 1030E SM2340B SM2320B SM2320B EPA350.1 EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540 C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA 200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1197 Preparation Date/Time 5/5/22 5/5/22 5/5/22 5/5/22 4/16/22 4/16/22 4/25/22 4/19/22 5/4/22 4/21/22 4/18/22 4/18/22 5/5/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/25/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22Dl197-04 Analysis Date/Time 5/24/22 5/24/22 5/24/22 5/24/22 4/16/22 4/16/22 4/25/22 4/19/22 5/4/22 4/21/22 4/19/22 4/18/22 5/24/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 Page 9 of 44 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 tA60RATOAIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-25_04122022 (cont.) Matrix: Water Date Sampled: 4/12/22 10:55 \ I ctal, ( l'OII I.) Uranium, Dissolved 0.0066 \ olatill-( lrl(,lllil· ( 01111H1111Hb Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 6/2/2022 Amended Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting Limit 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 15030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260015030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22D1197 Preparation Date/Time 4/26/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 Lab ID : 22D1197-04 Analysis Date/Time 4/26/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 J-LOW J-LOW J-LOW Page 10 of 44 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 13, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-25 04122022 576962004 Ground Water 12-APR-22 10:55 19-APR-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.210 The following Analytical Methods were performed: -------- MDC 0.698 RL 1.00 Project: Client ID: DNMI00100 DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/10/22 1735 2261341 Method Descri tion _____________ A_n_alyst Comments EPA 903.0 Surrog_ate/Tracer Recovert Test __ _ Nominal Recovery% Acceptable Limits ---------Result Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 10 l (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 16 of25 SDG: 576962 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l/~BORI\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-26_04202022 Matrix: Water Date Sampled: 4/20/22 14:00 ( akulation, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio I n••r1!an il· Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \lctal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 42.4 -0.04 42.4 0.94 318 < 1.0 0.4 56.8 0.2 0.8 1710 2560 2720 < 0.0050 < 0.0005 0.0006 445 < 0.0250 <0.010 < 0.0100 0.30 < 0.0010 164 0.965 < 0.0005 < 0.0100 < 0.0200 11.1 0.0085 <0.010 146 < 0.0005 < 0.10 < 0.0150 < 0.01 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 50.0 0.1 0.1 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/22/22 13:30@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030E SM !030E SM2340B SM2320B SM2320B EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540 C SM2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1691 Preparation Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 4/27/22 5/3/22 4/25/22 4/27/22 4/25/22 5/17/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Lab ID: 22D1691-09 Analysis Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 4/27/22 5/3/22 4/25/22 4/27/22 4/25/22 5/24/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/3/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Page 19 of 50 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA80RATORIES Energy Fuels Resources, Inc. Tanner Holllday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-26_04202022 (cont.) Matrix: Water Date Sampled: 4/20/22 14:00 ,Jctals (l'OIII.) Uranium, Dissolved 0.0514 \ olalil,· 01·l,!a11u· ( 11111pou111h Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform 447 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0025 20.0 1.0 1.0 10.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22D1691 Preparation Date/Time 5/2/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22Dl691-09 Analysis Date/Time 5/2/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 A-01 Page 20 of50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company : Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-26 04272022 578558008 Ground Water 27-APR-22 09:45 03-MAY-22 Client ----Project: Client ID: Report Date: May 26, 2022 DNMI00100 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method ------------------- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.308 0.636 1.00 pCi/L JXC9 05/24/22 1311 2268525 The following Analytical Methods were performed: _M_e_t_h_od _______ D_es_c_n~·p_ti_o_n ____________________ A_n_a_lyst Comments EPA 903.0 Surrogate/Tracer Recovery Test Result Nominal Recove~% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 107 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 20 of 22 SDG: 578558 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Forii Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 LABO~,\TORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-27_04122022 Matrix: Water Date Sampled: 4/12/22 11:15 ("akulatiom Anions, Total Cation/Anion Balance Cations, Total lnor1::111ir Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia asN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated \kral, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved Uranium, Dissolved \ olatill' 01·1:1111il· ( ompotrrHI, 11.5 4.4 12.5 230 < 1.0 < 0.05 31.7 0.9 6.3 327 728 < 0.0050 < 0.0005 < 0.0005 110 < 0.0250 <0.010 < 0.0100 <0.03 < 0.0010 47.0 < 0.0100 < 0.0005 <0.0100 < 0.0200 3.9 0.0160 <0.010 70.6 < 0.0005 < 0.10 < 0.0150 <0.01 0.0127 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 5.0 0.5 0.5 5.0 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 O.o3 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 0.0005 PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM 1030E SM 1030E SM 1030E SM 2320B SM 2320 B EPA 350.1 EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 CtF WO#: 22D1197 Preparation Date/Time 5/5/22 5/5/22 5/5/22 4/16/22 4/16/22 5/5/22 4/19/22 4/18/22 4/21/22 4/18/22 5/5/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/25/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22Dl197-05 Analysis Date/Time 5/24/22 5/24/22 5/24/22 4/16/22 4/16/22 5/5/22 4/19/22 4/19/22 4/21/22 4/19/22 5/24/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 Page 11 of 44 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA&OAATOIIIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-27_04122022 (cont.) Matrix: Water Date Sampled: 4/12/22 11:15 Volatik Or:,:a111<· ( om pound~ (con I.) Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 6/2/2022 Amended Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting Limit 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 2201197 Preparation Date/Time 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 Lab ID: 22D1197-05 Analysis Date/Time 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 J-LOW J-LOW J-LOW Page 12 of 44 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lld3:0AATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-27_05162022 Matrix: Water Date Sampled: 5/16/22 11 :50 ( alr11lali11m TDS Ratio 1111,r~anir Total Dissolved Solids (TDS) 1.0 748 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com None mg/L Certificate of Analysis PO#: Receipt: 5/18/22 12:20@ 0.8 °C Date Reported: 6/3/2022 Amended Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 20 Sampled By: Tanner Holliday SM 2340B SM2540C CtF WO#: 22E1503 Preparation Date/Time 6/2/22 5/19/22 Lab ID: 22El503-03 Analysis Date/Time 6/2/22 5/19/22 Page 7 of24 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 13, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW ---------Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW-27 04122022 576962005 Ground Water 12-APR-22 11:15 19-APR-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 1.18 +/-0.374 The following Analytical Methods were performed: Method Description ____ _ EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.913 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIOOIOO DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/10/22 1735 2261341 Analyst Comments Result Nominal Recovery% Acceptable Limits 98.4 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 17 of25 SDG: 576962 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/160/itATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-28_04192022 Matrix: Water Date Sampled: 4/19/22 14:45 ( ak11la11011, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio ln,1r~an;L. Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 50,7 -2.8 48.0 1.0 144 < 1.0 <0.05 130 0.4 5.1 2150 3320 3260 0.0101 < 0.0005 0.0040 436 < 0.0250 0.025 < 0.0100 < O.o3 < 0.0010 171 1.10 < 0.0005 < 0.0100 < 0.0200 10.7 0.0198 < 0.010 274 0.0009 < 0.10 < 0.0150 0.04 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 50.0 0.1 0.1 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/22/22 13:30@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030£ SM 1030 E SM 1030 E SM2340 B SM2320B SM2320B EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1691 Preparation Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 4/27/22 5/2/22 4/25/22 4/27/22 4/25/22 5/17/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Lab ID: 2201691-07 Analysis Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 4/27/22 5/2/22 4/25/22 4/27/22 4/25/22 5/24/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/3/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Page 15 of 50 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA601i:~\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-28_04192022 (cont.) Matrix: Water Date Sampled: 4/19/22 14:45 \ktals (runt.) Uranium, Dissolved 0.0101 \ olat11l-Orl,!anu· ( 11111pou11tl, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0025 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A CtF WO#: 2201691 Preparation Date/Time 5/2/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 2201691-07 Analysis Date/Time 5/2/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 A-01 Page 16 of 50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW --------------------~-----Client Sample ID: MW-28 04192022 Sample ID: 577764007 Matrix: Ground Water Collect Date: 19-APR-22 14:45 Receive Date: 26-APR-22 Collector: Client Project: Client ID: Report Date: May 23, 2022 DNMIOOlOO DNMIOOl Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method ----Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.280 0.782 1.00 pCi/L JXC9 05/18/22 1315 2265414 The following Analytical Methods were perform_e_d._· __ Method~-Descri lion __________________ _ EPA 903.0 -------~nJllyst Comments _ Surrogate/Tracer Recovery Barium Carrier Test Result Nominal Recov~~% Acceptable Limit~ GFPC, Total Alpha Radium, Liquid "As Received" 106 (25o/o-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows : DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 20 of27 SDG: 577764 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lABO~!.TORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-29_04142022 Matrix: Water Date Sampled: 4/14/22 10:05 ( aln1lali11m Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia asN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 59.0 -4.5 53.9 I.I 307 < 1.0 0.4 34.2 0.8 0.1 2550 4000 3780 < 0.0050 < 0.0005 < 0.0005 410 < 0.0250 <0.010 < 0.0100 1.05 < 0.0010 199 5.03 < 0.0005 < 0.0100 < 0.0200 15.2 < 0.0050 <0.010 383 < 0.0005 < 0.10 < 0.0150 < 0.01 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.2 5.0 0.5 0.1 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM 1030E SM 1030E SM !030E SM2340B SM 2320 B SM 2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1197 Pre pa ration Date/Time 5/5/22 5/5/22 5/5/22 5/5/22 4/16/22 4/16/22 4/25/22 4/19/22 4/18/22 4/21/22 4/18/22 4/19/22 5/5/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/25/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22Dl197-10 Analysis Date/Time 5/24/22 5/24/22 5/24/22 5/24/22 4/16/22 4/16/22 4/25/22 4/19/22 4/19/22 4/21/22 4/19/22 4/19/22 5/24/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 Page 21 of44 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA60A,\T0RlfS Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-29_04142022 (cont.) Matrix: Water Date Sampled: 4/14/22 10:05 \lctal, ( n,111.) Uranium, Dissolved 0.0157 \ olatil,· Ori.:anu· ( ompourHI, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 6/2/2022 Amended Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting Limit 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22D1197 Preparation Date/Time 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 2201197-10 Analysis Date/Time 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 J-LOW J-LOW J-LOW Page 22 of 44 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 13, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-29 04142022 576962010 Ground Water 14-APR-22 10:05 19-APR-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.219 The following Analytical Methods were performed: Method DescriQtion EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.869 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMI00100 DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/10/22 1736 2261341 Anal st Comments Result Nominal Recovery% Acceptable Limits ------109 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 22 of 25 SDG: 576962 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA&O~,\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-30_04202022 Matrix: Water Date Sampled: 4/20/22 11:40 C alr11la11011, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 21.9 -1.4 21.3 1.0 160 < 1.0 < 0.05 173 0.3 17 693 1400 1360 < 0.0050 < 0.0005 < 0.0005 234 < 0.0250 < 0.010 < 0.0100 < 0.03 < 0.0010 68.4 < 0.0100 < 0.0005 < 0.0100 < 0.0200 6.1 0.0649 <0.010 88.5 < 0.0005 < 0.10 < 0.0150 < 0.01 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 50.0 0.1 0.5 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030E SM 1030E SM 23408 SM23208 SM2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540C SM 2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1691 Preparation Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 4/27/22 5/3/22 4/25/22 4/27/22 4/25/22 5/17/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Lab ID: 22Dl691-10 Analysis Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 4/27/22 5/3/22 4/25/22 4/27/22 4/25/22 5/24/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/3/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Page 21 of 50 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA601lATOIIIE$ Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-30_04202022 (cont.) Matrix: Water Date Sampled: 4/20/22 11 :40 \lc1:1I, ( ,·11111.) Uranium, Dissolved 0.0096 \ 11l:1tik C )ri.:an1,· C ompouml, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofonn < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30 @ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0025 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22D1691 Preparation Date/Time 5/2/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 2201691-10 Analysis Date/Time 5/2/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 A-01 Page 22 of 50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 23, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: ---Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-30 04202022 577764010 Ground Water 20-APR-22 11 :40 26-APR-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.180 The following Analytical Methods were performed: --- MDC 0.532 RL Project: Client ID: DNMI00100 DNMI001 Units PF DF Analyst Date Time Batch Method ---- 1.00 pCi/L JXC9 05/18/22 1315 2265414 Method Descri_ption=-=----------~-___________ Analyst Comments EPA 903.0 Surrog;ate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 106 (25o/o-l25%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 22 of 27 SDG: 577764 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA60RATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-31_04112022 Matrix: Water Date Sampled: 4/11/22 13:45 ('akula111111, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio ln,,n!anir Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \kral, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 37.7 -0.5 37.6 1.9 164 < 1.0 < 0.05 372 0.5 18 1180 4300 2300 < 0.0050 < 0.0005 < 0.0005 351 < 0.0250 <0.010 < 0.0100 < 0.03 < 0.0010 177 < 0.0100 < 0.0005 <0.0100 < 0.0200 7.6 0.0989 < 0.010 117 < 0.0005 < 0.10 < 0.0150 < 0.01 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 20.0 0.1 0.5 20.0 500 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM 1030E SM 1030E SM 1030 E SM2340B SM2320B SM2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1197 Preparation Date/Time 5/5/22 5/5/22 5/5/22 5/5/22 4/16/22 4/16/22 5/5/22 4/19/22 4/18/22 4/21 /22 4/18/22 4/18/22 5/5/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/25/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 2201197-01 Analysis Date/Time 5/24/22 5/24/22 5/24/22 5/24/22 4/16/22 4/16/22 5/5/22 4/19/22 4/18/22 4/21/22 4/19/22 4/18/22 5/24/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 Page 3 of 44 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 llo.801V\T0RIE5 Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-31_04112022 (cont.) Matrix: Water Date Sampled: 4/11/22 13:45 \lctal, (ront.) Uranium, Dissolved 0.0220 \ olatik Or!!allll' ( ·0111po11111l, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 6/2/2022 Amended Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting !Jmi! 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22D1197 Preparation Date/Time 4/26/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 Lab ID: 22D1197-01 Analysis Date/Time 4/26/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 J-LOW J-LOW J-LOW Page 4 of 44 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 13, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard ---- Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-31_04112022 576962001 Ground Water I 1-APR-22 13:45 19-APR-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.294 The following Analytical Methods were perfonned: ---- Method Descri tion -~---------EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.770 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMI00100 DNMIOOI Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/10/22 1735 2261341 Aniili'.st Comments Result Nominal Recovery% Acceptable Limits 106 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 13 of25 SDG: 576962 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 ll,60~ATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-32_04112022 Matrix: Water Date Sampled: 4/11/22 12:45 ( ·alrulation, Anions, Total Cation/Anion Balance Cations, Total l11t1r:,!;anit.· Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated \ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved Uranium, Dissolved \ olatik Oq:a11i1· ( 0111po1111l1, 48.1 2.1 50.1 283 < 1.0 0.5 28.6 0.1 < 0.1 2050 3160 < 0.0050 < 0.0005 0.0018 479 < 0.0250 0.036 < 0.0100 4.02 < 0.0010 194 4.50 < 0.0005 0.0106 0.0439 13.0 < 0.0050 <0.010 223 < 0.0005 < 0.10 < 0.0150 0.06 0.0019 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.2 5.0 0.1 0.1 50.0 5 0.0050 0.0005 0.0005 2.0 0.0250 0.010 0.0100 0.20 0.0010 2.0 0.0100 0.0005 0.0100 0.0200 5.0 0.0050 0.010 5.0 0.0005 0.10 0.0150 0.01 0.0005 PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030E SM 1030E SM2320B SM2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.J EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 CtF WO#: 2201197 Preparation Date/Time 5/5/22 5/5/22 5/5/22 4/16/22 4/16/22 4/25/22 4/18/22 4/18/22 4/21/22 4/18/22 5/5/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/25/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 5/16/22 4/26/22 4/26/22 4/26/22 Lab ID: 22D1197-02 Analysis Date/Time 5/24/22 5/24/22 5/24/22 4/16/22 4/16/22 4/25/22 4/18/22 4/18/22 4/21/22 4/19/22 5/24/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 5/16/22 4/26/22 4/26/22 4/26/22 Page 5 of 44 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 l/\801'i<,\TORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-32_04112022 (cont.) Matrix: Water Date Sampled: 4/11/22 12:45 \olatilt· Orl(ann· ( ·,11npo11nd, (rnrll.l Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofonn < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 6/2/2022 Amended Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting Limit 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22D1197 Preparation Date/Time 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 Lab ID: 22Dl197-02 Analysis Date/Time 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 J-LOW J-LOW J-LOW Page 6 of44 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATOAIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-32_05162022 Matrix: Water Date Sampled: 5/16/22 12:20 ( alrnlation, TDS Ratio ln11rl,!anir Total Dissolved Solids (TDS) 1.0 3210 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com None mg/L Certificate of Analysis PO#: Receipt: 5/18/22 12:20@ 0.8 ·c Date Reported: 6/3/2022 Amended Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 20 Sampled By: Tanner Holliday SM 2340 B SM 2540 C CtF WO#: 22E1503 Preparation Date/Time 6/2/22 5/19/22 Lab ID: 22El503-04 Analysis Date/Time 6/2/22 5/19/22 Page 8 of 24 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 13, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW ------------------Client Sample ID: MW-32 04112022 Sample ID: 576962002 Matrix: Ground Water Collect Date: I 1-APR-22 12:45 Receive Date: 19-APR-22 Collector: Client -------- Parameter Qualifi~ Result Uncertainty ~DC Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 1.82 +/-0.445 0.841 The following Analytical Methods were perfonned: ---------Method Descri tion EPA 903.0 Surrogate/Tracer Recovery Test Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMI00100 DNMIOOI Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/10/22 1735 2261341 Analyst Comments Result Nominal Recovery% ~cceptable Limit~ 107 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 14 of 25 SDG: 576962 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-35_04122022 Matrix: Water Date Sampled: 4/12/22 14:20 ( alculation, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio ln(1rgani,: Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 52.3 -2.9 49.4 1.4 252 < 1.0 < 0.05 63.5 0.3 <0.1 2230 4800 3390 < 0.0050 < 0.0005 < 0.0005 451 < 0.0250 < 0.010 < 0,0100 0.20 < 0.0010 149 0.241 < 0.0005 < 0.0100 < 0.0200 10.7 0.0064 <0.010 330 < 0.0005 < 0.10 < 0.0150 < 0.01 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 5.0 0.1 0.1 50.0 500 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0,0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM 1030E SM 1030 E SM 1030E SM2340B SM2320B SM2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200,8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1197 Preparation Date/Time 5/5/22 5/5/22 5/5/22 5/5/22 4/16/22 4/16/22 4/25/22 4/19/22 5/4/22 4/21/22 4/18/22 4/18/22 5/5/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/25/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 2201197-06 Analysis Date/Time 5/24/22 5/24/22 5/24/22 5/24/22 4/16/22 4/16/22 4/25/22 4/19/22 5/4/22 4/21/22 4/19/22 4/18/22 5/24/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 A-01 Page 13 of 44 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l1'80R,\TOPIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-35_04122022 (cont.) Matrix: Water Date Sampled: 4/12/22 14:20 \lctal, (n111t.J Uranium, Dissolved 0.0211 \ olatik Oq:anu· < ompoumls Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 6/2/2022 Amended Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting Limit 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22D1197 Preparation Date/Time 4/26/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 Lab ID: 2201197-06 Analysis Date/Time 4/26/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 4/25/22 J-LOW J-LOW J-LOW Page 14 of 44 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 13, 2022 Company: Address : Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill G W ----MW-35 04122022 576962006 Ground Water 12-APR-22 14:20 19-APR-22 Client Project: Client ID: DNMI00100 DNMI001 ---------- P.arameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method ------ Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 3. 75 +/-0.560 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Test 0.756 1.00 Surrogate/Tracer Recovery Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). pCi/L JXC9 05/10/22 1735 2261341 An~)y_s! Comments Result Nominal Recovery% Acceptable Limits 102 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 18 of 25 SDG: 576962 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lft80R,\TOA:IES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-36_04212022 Matrix: Water Date Sampled: 4/21/22 7:40 { ak11la1111n, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnorgank Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \lct:il, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 59.3 -1.8 57.2 0.98 273 < 1.0 <0.05 54.6 0.3 0.2 2560 3890 3940 < 0.0050 < 0.0005 < 0.0005 354 < 0.0250 < 0.010 < 0.0100 0,07 < 0.0010 121 < 0.0100 < 0.0005 < 0.0100 < 0.0200 8.8 0.256 <0.010 674 0.0006 < 0.10 < 0.0150 < 0.01 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting !d.!!!l! 1.0 1.0 0.05 5.0 0.1 0.1 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 2.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/22/22 13:30@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030E SM 1030E SM2340B SM 2320 B SM2320 B EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1691 Preparation Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 5/3/22 5/19/22 4/25/22 4/27/22 4/25/22 5/17/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Lab ID: 2201691-12 Analysis Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 5/3/22 5/19/22 4/25/22 4/27/22 4/25/22 5/24/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/3/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Page 25 of 50 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 tA80ijo\TORlf.S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-36_04212022 (cont.) Matrix: Water Date Sampled: 4/21/22 7:40 \klab, (l'OIII.) Uranium, Dissolved 0.0228 \ ulatik ( )q!,11111· ( 11111p1111111I, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chi oromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 l.O 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22D1691 Preparation Date/Time 5/2/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 2201691-12 Analysis Date/Time 5/2/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 A-01 Page 26 of50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 23, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW ----------CI i en t Sample ID: MW-36_04212022 Sample ID: 577764012 Matrix: Ground Water Collect Date: 2 l-APR-22 07:40 Receive Date: 26-APR-22 Collector: Client Parameter Qualifier Result Uncertainty MDC ---------- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.231 0.446 RL 1.00 The following Analytical Methods were performed: --=--------------Method Deseri tion EPA 903.0 Surrogate/Tracer Recovery Test Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). Project: Client ID: DNMI00100 DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/18/22 1315 2265414 Anal stCo=m=m~e=nt=s'----------~ Result Nominal Recovery% Acceptable Limits 107 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 24 of 27 SDG: 577764 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l/1BOFt!\TORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-37_05172022 Matrix: Water Date Sampled: 5/17/22 8:30 ( akulatiom Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnor~anil· Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ktal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 52.8 4.6 57.9 1.0 174 < 1.0 < 0.05 46.4 0.2 0.3 2340 3660 3640 < 0.0050 < 0.0005 < 0.0005 476 < 0.0250 <0.010 < 0.0100 < 0.10 < 0.0010 135 < 0.0100 < 0.0005 < 0.0100 < 0.0200 15.5 0.0070 <0.010 521 0.0006 < 0.10 < 0.0150 0.02 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 1.0 0.1 0.1 100 20 5 0.0050 0.0005 0.0005 1.0 0.0250 0.010 0.0100 0.10 0.0010 1.0 0.0100 0.0005 0.0100 0.0200 2.5 0.0050 0.010 2.5 0.0002 0.10 0.0150 0.01 PO#: Receipt: 5/18/22 12:20@ 0.8 °C Date Reported: 6/3/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030 E SM 1030£ SM2340 B SM2320 B SM2320 B EPA350.1 EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22E1503 Preparation Date/Time 6/2/22 6/2/22 6/2/22 6/2/22 5/24/22 5/24/22 5/27/22 5/25/22 5/25/22 5/24/22 5/31/22 5/19/22 6/2/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/18/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 Lab ID: 22E1503-02 Analysis Date/Time 6/2/22 6/2/22 6/2/22 6/2/22 5/24/22 5/24/22 5/27/22 5/25/22 5/25/22 5/24/22 5/31/22 5/19/22 6/2/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/20/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 5/27/22 Page 5 of 24 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the Jntermountain West Since 1953 LAB0~ATOAIE5 Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-37_05172022 (cont.) Matrix: Water Date Sampled: 5/17/22 8:30 ,1c1a1, (runt.) Uranium, Dissolved 0.0115 , ol.1tik ()q:a111r ( ·0111po111HI, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 5/18/22 12:20@ 0.8 ·c Date Reported: 6/3/2022 Amended Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22E1503 Preparation Date/Time 5/27/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 Lab ID: 22E1503-02 Analysis Date/Time 5/27/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 J-LOW J-LOW Page 6 of 24 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: June 16, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW -------~ Client Sample ID: MW-37 05172022 Sample ID: 580437002 Matrix: Ground Water Collect Date: 17-MA Y-22 08:30 Receive Date: 19-MA Y-22 Collector: Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.290 The following Analytical Methods were performed: Method Descri J.!.Q!!_ EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.663 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMI00100 DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/24/22 1312 2268525 Analyst Comments Result Nominal Recovery% Accertable Limits 109 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 13 of 15 SDG: 580437 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA60R:ATOAIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-38_04272022 Matrix: Water Date Sampled: 4/27/22 10:30 ( akulatwn, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio ln11q~a11k Alkalinity· Bicarbonate (as CaC03) Alkalinity· Carbonate (as CaC03) Ammonia asN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 61.3 ·7.5 52.8 0.80 94.I < 1.0 < 0.05 39.9 0.8 14 2820 3150 3920 < 0.0050 < 0.0005 < 0.0005 428 < 0.0250 < 0.010 < 0.0100 < 0.03 < 0.0010 175 < 0.0100 < 0.0005 < 0.0100 < 0.0200 23.7 0.175 < 0.010 377 < 0.0002 < 0.10 < 0.0150 <0.01 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0,05 20.0 0.1 0.1 20.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0002 0.10 0.0150 0.01 PO#: Receipt: 4/29/22 11 :00@ 0.0 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030 E SM 1030E SM2340 B SM2320B SM 23208 EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA 200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 2202139 Preparation Date/Time 5/27/22 5/27/22 5/27/22 5/27/22 5/3/22 5/3/22 5/11/22 5/7/22 5/4/22 4/29/22 5/7/22 5/2/22 5/27/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/2/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 Lab ID: 22D2139-06 Analysis Date/Time 5/27/22 5/27/22 5/27/22 6/1/22 5/3/22 5/3/22 5/12/22 5/8/22 5/4/22 4/30/22 5/8/22 5/2/22 6/1/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/4/22 5/10/22 5/10/22 5/10/22 5/10/22 5/10/22 5/11/22 5/10/22 5/10/22 5/10/22 5/10/22 Page 13 of 35 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 ,1.e;Q.&t l\TOR1t:.'S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-38_04272022 (cont.) Matrix: Water Date Sampled: 4/27/22 10:30 \)dais (runt.) Uranium, Dissolved 0.0064 \ ulatill· Organ1r ( 11111p1111111h Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/29/22 11 :00@ o.o ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0003 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A CtF WO#: 22D2139 Preparation Date/Time 5/10/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 Lab ID: 2202139-06 Analysis Date/Time 5/10/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 A-01 Page 14 of 35 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 26, 2022 Company: Address : Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-38 04272022 578558006 Ground Water 27-APR-22 10:30 03-MAY-22 Client Parameter Qualifier Result Uncerta_in--'ty~ __ M_D_C_ Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.223 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Surrogate/Tracer Recovery Test 0.502 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIOOIOO DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/24/22 1311 2268525 _f\nalyst Comments Result Nominal Recovery% Acceptable Limits 111 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 18 of 22 SDG: 578558 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Ll,BORATOll:IES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-39_04202022 Matrix: Water Date Sampled: 4/20/22 11:00 ( akulalions Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \let.ti, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 60.2 -4.5 55.0 I.I < 1.0 < 1.0 0.3 39.9 0.6 0.1 2840 4260 3950 <0.0050 0.0053 0.0024 351 < 0.0250 0.056 0.0197 11.8 < 0.0010 167 2.03 < 0.0005 < 0.0100 0.0292 12.6 0.0060 <0.010 523 0.0037 <0.10 < 0.0150 0.16 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 5.0 0.5 0.1 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 2.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/22/22 13:30@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030 E SM 1030 E SM 2340B SM 23208 SM2320 B EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 2201691 Preparation Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 515122 5/3/22 5/3/22 4/25/22 4/27/22 4/25/22 5/17/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Lab ID: 22Dl691-ll Analysis Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/24/22 4/24/22 5/5/22 5/3/22 5/3/22 4/25/22 4/27/22 4/25/22 5/24/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/3/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Page 23 of 50 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/d.!.OR,,TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-39_04202022 (cont.) Matrix: Water Date Sampled: 4/20/22 11:00 \lctals I cont.) Uranium, Dissolved 0.0115 \ olatilr Orl(anll' < ompou1uh Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Ch I oromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22D1691 Preparation Date/Time 5/2/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22D1691-11 Analysis Date/Time 5/2/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 A-01 Page 24 of 50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 23, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-39 04202022 577764011 Ground Water 20-APR-22 11 :00 26-APR-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 1.36 +/-0.299 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.504 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIOOlOO DNMIOOl Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/18/22 1315 22654 I 4 Analyst Comments Result Nominal Recovery% Acceptable Limits 109 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 23 of27 SDG: 577764 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-40_04192022 Matrix: Water Date Sampled: 4/19/22 13:50 c·akulation, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio I nor~anil' Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 48.4 -6.6 42.4 1.1 220 < 1.0 0.05 39.6 0.5 2.2 2100 3300 3060 < 0.0050 < 0.0005 < 0.0005 345 < 0.0250 <0.010 < 0.0100 < 0.03 < 0.0010 158 0.0958 < 0.0005 < 0.0100 < 0.0200 7.4 0.178 < 0.010 276 < 0.0005 <0.10 < 0.0150 <0,01 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting !d!!!i.! 1.0 1.0 0.05 5.0 0.5 0.1 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030E SM 1030E SM2340B SM2320B SM2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1691 Preparation Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 5/2/22 5/2/22 4/25/22 4/27/22 4/25/22 5/17/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Lab ID: 22D1691-08 Analysis Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 5/2/22 5/2/22 4/25/22 4/27/22 4/25/22 5/24/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/3/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Page 17 of 50 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 ll~60R~\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-40_04192022 (cont.) Matrix: Water Date Sampled: 4/19/22 13:50 \lct:tl, (cunt.) Uranium, Dissolved 0.0229 \'olatill· Orcanir ( umpoumls Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0025 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22D1691 Preparation Date/Time 5/2/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 Lab ID: 2201691-08 Analysis Date/Time 5/2/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 4/27/22 A-01 Page 18 of 50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 23, 2022 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-40 04192022 577764008 Ground Water 19-APR-22 13:50 26-APR-22 Client Parameter Qualifier Result Uncertainty ----------Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.274 The following Analytical Methods were performed: Method Descri tion EPA 903.0 MDC 0.684 Surrogate/Tracer Recovery Test ~~----------------8 a r i um Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMI00100 DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/18/22 1315 2265414 Analyst Comments Result Nominal Recovery% Acceptable .!:imit~ 105 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 21 of27 SDG: 577764 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lABor,rnTORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: TW4-24_04272022 Matrix: Water Date Sampled: 4/27/22 12:30 ( akulaliom Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnor~anit· Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \ll'tal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 122 0.9 124 0.94 915 < 1.0 12.6 1200 0.5 47 3500 7220 7680 < 0.0050 < 0.0005 0.0006 544 < 0.0250 < 0.010 < 0.0100 < 0.04 < 0.0010 379 0.426 < 0.0005 1.38 < 0.0200 10.5 0.0715 <0,010 1500 0.0027 <0.10 < 0.0150 < O.oI Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 1.2 100 0.1 0.1 100 20 5 0.0050 0.0005 0.0005 0.4 0.0250 0.010 0.0100 0.04 0.0010 0.4 0.0100 0.0005 0.0100 0.0200 1.0 0.0050 0.010 1.0 0.0005 0.10 0.0150 O.oJ PO#: Receipt: 4/29/22 11 :00@ 0.0 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030E SM 1030E SM 23408 SM 23208 SM 2320 B EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D2139 Preparation Date/Time 5/27/22 5/27/22 5/27/22 5/27/22 5/3/22 5/3/22 5/11/22 5/7/22 5/4/22 4/29/22 5/7/22 5/2/22 5/27/22 5/4/22 5/4/22 5/4/22 5/9/22 5/4/22 5/4/22 5/4/22 5/9/22 5/4/22 5/9/22 5/4/22 5/2/22 5/4/22 5/4/22 5/9/22 5/4/22 5/4/22 5/9/22 5/4/22 5/9/22 5/4/22 5/4/22 Lab ID: 2202139-07 Analysis Date/Time 5/27/22 5/27/22 5/27/22 6/1/22 5/4/22 5/4/22 5/12/22 5/8/22 5/4/22 4/30/22 5/8/22 5/2/22 6/1/22 5/5/22 5/5/22 5/5/22 5/10/22 5/5/22 5/5/22 5/5/22 5/11/22 5/5/22 5/10/22 5/5/22 5/4/22 5/5/22 5/5/22 5/10/22 5/5/22 5/5/22 5/11/22 5/5/22 5/10/22 5/5/22 5/5/22 Page 15 of 35 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lt.60~ATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: TW4-24_04272022 (cont.) Matrix: Water Date Sampled: 4/27/22 12:30 \lcrals (rnnl.) Uranium, Dissolved 1.04 \ olalih· Or!!anir ( 11mp111111tls Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofonn 5.4 Chloromethane < 1.0 Methyl Ethyl Ketone < 20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/29/22 11 :OO@ o.o ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 l.O 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A CtF WO#: 22D2139 Preparation Date/Time 5/4/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 Lab ID: 22D2139-07 Analysis Date/Time 5/5/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 A-01 Page 16 of 35 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 26, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW TW4-24 04272022 578558007 Ground Water 27-APR-22 12:30 03-MAY-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.278 The following Analytical Methods were performed: ---- MDC 0.762 RL 1.00 Project: Client ID: DNMI00100 DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/24/22 1311 2268525 Method Descri tion _____________ Anal st Comments __ _ EPA 903.0 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits ------Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 116 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 19 of22 SDG: 578558 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Ll1BOR:~\TORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-65_04142022 Matrix: Water Date Sampled: 4/14/22 10:05 C ah-ulation, Anions, Total Cation/Anion Balance Cations, Total IDS Ratio lnoruanir Alkalinity -Bicarbonate (as CaC03) Alkalinity· Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (IDS) IDS, Calculated Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 59.0 -3.6 55.0 1.1 307 < 1.0 0.6 34.4 0.5 < 0.1 2550 4070 3800 <0.0050 < 0.0005 < 0.0005 415 < 0.0250 <0.010 < 0.0100 1.09 < 0.0010 202 5.02 < 0.0005 < 0.0100 < 0.0200 15.7 < 0.0050 < 0.010 395 < 0.0005 < 0.10 < 0.0150 < 0.01 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.2 5.0 0.5 0.1 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM 1030E SM 1030 E SM 1030 E SM2340B SM2320B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM 2540 C EPA200.8 EPA200.8 EPA 200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1197 Preparation Date/Time 5/5/22 5/5/22 5/5/22 5/5/22 4/16/22 4/16/22 4/25/22 4/19/22 4/18/22 4/21/22 4/18/22 4/19/22 5/5/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/25/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22D1197-11 Analysis Date/Time 5/24/22 5/24/22 5/24/22 5/24/22 4/16/22 4/16/22 4/25/22 4/19/22 4/19/22 4/21/22 4/19/22 4/19/22 5/24/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 4/26/22 4/26/22 4/27/22 4/26/22 4/26/22 4/27/22 4/26/22 4/27/22 4/26/22 4/26/22 Page 23 of 44 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 l/\80fil,\TCI fl I ES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-65_04142022 (cont.) Matrix: Water Date Sampled: 4/14/22 10:05 \ktal, (rnnt.l Uranium, Dissolved 0.0155 \ olatik (hganu· ( 0111pou111I, Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 6/2/2022 Amended Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting !d!!!i! 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A CtF WO#: 22D1197 Preparation Date/Time 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22D1197-11 Analysis Date/Time 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 J-LOW J-LOW J-LOW Page 24 of44 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 13, 2022 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-65 04142022 576962011 Ground Water 14-APR-22 10:05 19-APR-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha u 1.00 +/-0.197 The following Analytical Methods were performed: Method DescriQtion EPA 903.0 Surrogate/Tracer Recovef)'.' Test MDC 0.815 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (l-sigma). RL 1.00 Project: Client ID: Units PF pCi/L DNMIOOIOO DNMI001 DF Analyst Date JXC9 05/10/22 Anal st Comments Result Nominal Recovery% 108 Time Batch Method 1736 2261341 Acceptable Limits (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 23 of25 SDG: 576962 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/\60RATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-70_04212022 Matrix: Water Date Sampled: 4/21/22 7:40 ( 'aln1lat1om Anions, Total Cation/Anion Balance Cations, Total TDS Ratio ln11r:!ank Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) TDS, Calculated \kcal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Vanadium, Dissolved Zinc, Dissolved 58.9 -1.0 57.8 0.90 252 < 1.0 < 0.05 55.0 0.3 0.3 2560 3540 3940 < 0.0050 < 0.0005 < 0.0005 359 < 0.0250 <0.010 < 0.0100 < 0.03 < 0.0010 122 < 0.0100 < 0.0005 < 0.0100 < 0.0200 8.9 0.263 <0.010 680 0.0006 < 0.10 < 0.0150 <0.01 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.05 5.0 0.1 0.1 50.0 20 5 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0,03 0.0010 0.2 0.0100 0.0005 0.0100 0.0200 0.5 0.0050 0.010 2.5 0.0005 0.10 0.0150 0.01 PO#: Receipt: 4122122 13:30@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030E SM 1030E SM2340B SM2320B SM2320 B EPA350.l EPA300.0 EPA300.0 EPA 353.2 EPA300.0 SM 2540 C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22D1691 Preparation Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 5/3/22 5/19/22 4/25/22 4/27/22 4/25/22 5/17/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Lab ID: 2201691-13 Analysis Date/Time 5/17/22 5/17/22 5/17/22 5/17/22 4/23/22 4/23/22 5/5/22 5/3/22 5/19/22 4/25/22 4/27/22 4/25/22 5/24/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/3/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 5/2/22 Page 27 of 50 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LM\O~ATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-70_04212022 (cont.) Matrix: Water Date Sampled: 4/21/22 7:40 \Jrt:11, (rnnt.) Uranium, Dissolved 0.0232 \'olatill-Organll' ( ompnunll- Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 0.0005 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A CtF WO#: 2201691 Preparation Date/Time 5/2/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22D1691-13 Analysis Date/Time 5/2/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 A-01 Page 28 of 50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 23, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW ---------Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW-70_04212022 577764013 Ground Water 2 l-APR-22 07:40 26-APR-22 Client Parameter Qualifier Result Uncertainty Rad Gas Fl<?w Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.262 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.673 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIOOIOO DNMIOOI Units PF DF Analyst Date Time Batch Method pCi/L JXC9 05/18/22 1315 2265414 Result Nominal Recovery% Acceptable Limits 99.2 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 25 of 27 SDG: 577764 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 4/14/22 12:45 \ olatilt· Organ it· ( ompouruh Acetone Benzene Carbon Tetrachloride Chloroform Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total <20.0 < 1.0 < 1.0 < 1.0 < 1.0 <20.0 < 1.0 < LO < 1.0 < 1.0 < l.O Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 6/2/2022 Amended Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting Limit 20.0 1.0 1.0 1.0 1.0 20.0 l.O 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22D1197 Preparation Date/Time 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID: 22D1197-12 Analysis Date/Time 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 J-LOW J-LOW J-LOW Page 25 of44 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lABOR:>\TOIHfS Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 4/18/22 11:20 \ olat1ll· ( >ri.:anu· ( ompoumh Acetone Benzene Carbon Tetrachloride Chloroform Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total <20.0 < 1.0 < 1.0 < 1.0 < 1.0 <20.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/22/22 13:30@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22D1691 Preparation Date/Time 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 Lab ID : 2201691-14 Analysis Date/Time 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 4/26/22 A-01 Page 29 of 50 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/160R,\TOIIIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 4/25/22 12:50 \ olatilt· Or1!an1t· ( om pound, Acetone Benzene Carbon Tetrachloride Chloroform Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total <20.0 < 1.0 < 1.0 < 1.0 < 1.0 <20.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 4/29/22 11 :00@ 0.0 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22D2139 Preparation Date/Time 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 Lab ID: 2202139-08 Analysis Date/Time 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 5/3/22 A-01 Page 17 of 35 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 5/17/22 8:00 \'olalile Or~anil' ( ompoumh Acetone Benzene Carbon Tetrachloride Chloroform Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total <20.0 < 1.0 < 1.0 < 1.0 < 1.0 <20.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 5/18/22 12:20@ 0.8 °C Date Reported: 6/3/2022 Amended Project Name: 2nd Quarter Ground Water 2022 Minimum Reporting Limit 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22E1503 Preparation Date/Time 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 Lab ID: 22E1503-05 Analysis Date/Time 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 5/25/22 J-LOW J-LOW Page 9 of 24 9632 South 500 West CHEMTECH-FORD LABORATO~IES Amended 6/2/2022 Work Order: 2201197 Pro,ject: 2nd Quarter Groundwater 2022 Energy Fuels Resources, Inc. Attn: Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Client Service Contact: 801.262.7299 The analyses presented on this report were performed in accordance with the National Environmental Laboratory Accreditation Program (NELAP) unless noted in the comments, flags, or case narrative. If the report is to be used for regulatory compliance, it should be : presented in its entirety, and not be altered. Approved By: Melissa Connolly, Project Manager Sandy, Utah 84070 801 .262.7299 Main 866.792.0093 Fax Serving the /ntermountain West since 1953 www.ChemtechFord.com I CHEMTECH·FORD LABOFL~TORIES Energy Fuels Resources, Inc. Project: 2nd Quarter Groundwater 2022 Project Manager: Tanner Holliday Laboratory ID Sample Name 2201197-01 MW-31 _04112022 2201197-02 MW-32_04112022 2201197-03 MW-02_04122022 2201197-04 MW-25_04122022 2201197-05 MW-27 _04122022 2201197-06 MW-35_04122022 2201197-07 MW-18_04132022 2201197-08 MW-19_04132022 2201197-09 MW-01_04142022 2201197-10 MW-29_04142022 2201197-11 MW-65_04142022 2201197-12 Trip Blank Amended Work Order Report Narrative Amended Report Comments The sample ID for 2201197-06 has been corrected. The spike amounts, percent recoveries, and/or limits have been updated for method 82600 on the QC reports. Total Dissolved Solids Comments Due to laboratory error the samples were over-diluted for Total Dissolved Solids analysis on samples 2201197-01, -03, -04, -06, -07, and -08. The analytical results acquired for the Total Dissolved Solids have been determined to be inaccurate and biased high for these samples. The analysis could not be performed again within the holding time. The laboratory considers the TDS, Calculated to be a more accurate representation of the actual TDS for these samples . The TDS Ratio results are also biased for these samples. Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions The corrective action required with this workorder and the Total Dissolved Solids analysis included additional training on proper sample aliquot measuring and performing dilution. Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com CtF WO#: 22D1197 I CHEMTECH·FORD Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 l>\00111ATORIES Amended Certificate of Analysis PO#: 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Groundwater 2022 Report Footnotes Abbreviations ND = Not detected at the corresponding Minimum Reporting Limit (MRL). 1 mg/L = one milligram per liter or 1 mg/kg= one milligram per kilogram = J part per million. 1 ug/L = one microgram per liter or l uglkg = one microgram per kilogram= 1 part per billion. 1 ng/L = one nanogram per liter or I ng/kg = one nanogram per kilogram = I part per trillion. Flag Descriptions A-01 = This analyte was not detected and has been evaluated and reported to the MDL of 0.03 mg/L. J-LOW = Estimated low due to low recovery ofLCS or CCV Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com CtF WO#: 22D1197 Page 26 of 44 ~ [) C D 0 0 D American West Analytical Laboratories 463 W. 3600 S. Salt Lake City, UT 84115 Phone# (801) 263-a686 Toll Free# (888) 263-a686 L~ Fax# (801) 263-8667 Email awal@awaHabs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blandinc, UT 84511 Contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: Email: tholllday@e11eqyfaela.eom; KWeine~eneqyfaels.com Project Name: 2nd Quarter Ground water 2022 Project#: PO#: Sampler Name: Tanner Holliday 2ZD 1\91 Date SamolelD: Sampled I NW-31_04112022 4/11/2022 ~ IIIW-32_04112022 4/11/2022 j IIIW-02_04122022 4/12/2022 j IIIW-25_04122022 4/12/2022 l IIIW-27_04122022 4/12/2022 f IIW-35_04122022 4/12/2022 f IIW-18_04132022 4/13/2022 ~ IIW-19_04132022 4/13/2022 1 aw-01_04142022 4/14/2022 ~ IIW-29_04142022 4/14/2022 \ IIIW-6.5_04142022 4/14/2022 I~ TRIP BLANK 4/11/2022 by~~,••-I 1 J/ /;_ ale: '""'nature 4/14'?07. mme: """'Name: r.,.,.,..~--11"' lly. Date: l<:1nn.,iun, [Tlme: PrintNnme: lly. !Date: --nme: PtlnC Name:: Rellnqulshed by: Date: =nature rnme: ""'"'Nano, I Time Sampled 134$ 124S 1335 1055 1115 1420 1135 1335 945 1005 1005 124$ Received by: L<:innarun, CHAIN OF CUSTODY All analysis will be conducted using NELAP accredited methods and all data will be reported using AWAL's standard ana1yte IISls and reporting limils (POL) unless specilically requested olhe!Wise on lhis Chain of CUslody and/or attached documentation. "I QC Lewi: \ I Tum Around Time: Unless other arrangementll have been made, signed repo!IS wt!! be emaile<! by 5:00 pm on ... 3 Standard Ille day lhey are due . X Include EDD: 0 LOCUB UPLOAD ::;: "' u EXCEL bO 00 X Field Filtered For: -. ::c ::;: Dfaolnd Keblla ..., i:: lli ::;: :i ~ C'I .D af ~ a. z For CornpHance With: c .; s:: D NELAP 0 ~ N D RCRA o' C'I ;i > D CWA g ;:::_. c u -:::i D SDWA -. O') 0 D ELAP/A2LA ..., CQ' 0 c .. ~ u i::-Q D NLLAP lt) 0 rn ~ O') 0 C'I -! .: D Non-Compliance 0 O') C) 1= g .. lt) ~ ... D Other: Q ::t. " .,; "" G' e \'2. c:, G' 1 :a u < " 0 CD )( Cl .... 0 u IO -'= "S "' Cl ii ~ .! "Cl ,; .; -! C'I .!! .. 0 lt) lt) 1 co rn ~ C ::; I!: ::t. ~ 1111 Known Hazards 0 CD -0 -0 .,; z 1111 • 0 ci " "' ID = • < g & 0 E 0 ; t ~ i5 a .. I!: CJ 0 Samole Comments .. rJJ ... 7 w X X X X X X X X X X 7 w X X X ~ X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X I>-.. X X X X X X OWJ. ,l\oJ b:rn\.-CA. 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 3 w X '-J j y\ ,--...,.., 0 ~"rr.11.~) 0311!'.4 1 s l:2-2-Special Instructions: AWAL Lab Sample Set# Page 1 of 1 r=- Laboratory Use Only lsa,np1es Wen; t_.cfS ~-defiver..i 2 Aml)ient~ 3 Tem~ fil•c 4 Received Broken/1.Mking (lmproper1)' 5ealea) y N 5 Proper1yPn!served y N Checked al bench y N .. 6 R«.Jived Wllllln Hoking Times y N r.nr, Tape Was: 1 Present on Outer Package y N NA 2 Uroroken on Out..-Package y N NA 3 Present on Sanple y N NA 4 Unbroken on Sample y N NA Between Sanple ~ and COC Reconl? y N --~"so B ,t.1u~'\ 1nmet II lf'l ~ 'l.JO Sample containers for metals were field filtered. See the ReceMN!lly. l"'-nat1n Date; Analytical Scope of Work for Reporting Lim.its and voe analyte rrome: list. i:Mi .... Name: Received by: Date: • -Client will re-sample per Kathy 5/16 """"""-mme: 1A~ Pr1n1Namet ReceM>dby: !Date: ,-·--·,._....., .. ., ' L<:lnnatu,e TRACKING #: 1 Z 187 Y 4Y 03 9493 3454 mm•: 1 ....... Name: I Work Order# ZZDl I~] Delivery Method: CitUPS D USPS D FedEx D Chemtech courier D Walk-in D Customer Courier ~ .. .9 ·1 i ~ I i .. 'ii. i E C I .!! j Chemtech Lot# :s 'S l ·1 .. ) Sample# Container Preservative E i .f .; I-DI-II ~ M -AP A IV\ Wf-~'l --\z \JV r -:z. A,,, '-,/ ~ .. fii ;. .., .; u:: Misc s ... Volume ~ -~ (o,/mU CHEMTECH FORD LABORATORIES Sample Receipt Receiving Temperature O . 9 ·c Comments C' ~,~~~ , ·~ --"::O . ..:; ,.,-,,.J, \J\'a \ '-·""' ·~J'\ c-.\ .'o \ .rt CHEMTECH-FORO I, r'l. $ 0 R ,t., T (:;, q J :'. S Sample Condition ( check if yes-I ~ySeats 0 Containers Intact :::/1=5 Cif cote.an be matched to bottles Rectived on Ice ~rre<;t Containers(sl ifsufficent Sample Volume 0 Headspace Present (VOCI D Temperature Blank ~eceived within Holding Time Plastic Containers A· Plastic Ur,p<•"1V<><I 8· Miscellaneous Plastic C, Cyanide Qt INaOH) E· Co5fotm/!;c.oli;'HPC F· Sulfide Qt (Zn Acetate) L• Mercury 1631 ,M. Metals Pint (HN03} N Nutrient Pint (H2S04) R-Radiological IHN03J S• Sludge Cups/Tubs Q,. Pla~ic Bag Glass Containers 0-625 1Na2S203) G· Gl,»t, Unpreserved M, HAAs INH4CIJ 1· 508/515/5251Na2S03J iC • 515 3 HerbtCidec. 0· Oil & Grease (HCIJ p. Phenol, {H2S04) 11'· TOC(TOX (H3P04) U 531 IMCAA, Na25703) V 524trHMs (A.scorbic Acid) w. 8260 voe 11,1 HCIJ '\ Via! Unpreserved Y 524/504 INa25203) I M1sce!:aneous Glass v~\b~ Analyte QC Sample ID: BWD1104-BLKI Date Prepared: 04/26/2022 Calcium, Dissolved Iron, Dissolved Magnesium, Dissolved Potassium, Dissolved Sodium, Dissolved Tin, Dissolved QC Sample ID: BWD1105-BLKI Date Prepared: 04/26/2022 Calcium, Dissolved Iron, Dissolved Magnesium, Dissolved Potassium, Dissolved Sodium, Dissolved Tin, Dissolved QC Sample ID: BWE0724-BLKI Date Prepared: 05/16/2022 Tin, Dissolved QC Sample ID: BWD1104-BSI Date Prepared: 04/26/2022 Calcium, Dissolved Iron, Dissolved Magnesium, Dissolved Potassium, Dissolved Sodium, Dissolved Tin, Dissolved QC Sample ID: BWD1105-BSI Date Prepared: 04/26/2022 Calcium, Dissolved Iron, Dissolved Magnesium, Dissolved Potassium, Dissolved Sodium, Dissolved Tin, Dissolved QC Sample ID: BWE0724-BSI Date Prepared: 05/16/2022 Tin, Dissolved QC Sample ID: BWD1104-MSI Date Prepared: 04/26/2022 Calcium, Dissolved Iron, Dissolved Magnesium, Dissolved Potassium, Dissolved Sodium, Dissolved Tin, Dissolved CtF WO#: 22D1197 www.ChemtechFord.com QC Report for Work Order (WO) -22D1197 %Rec RPO Limits RPO Max Result Source Cone Blank-EPA 200.7 Batch: BWD1104 Date Analyzed: 04/26/2022 ND ND ND ND ND ND Batch: BWDI 105 Date Analyzed: 04/27/2022 ND ND ND ND ND ND Batch: BWE0724 Date Analyzed: 05/16/2022 ND LCS -EPA 200.7 Batch: BWD1104 Date Analyzed: 04/26/2022 96.2 85 -115 9.8 102 85-115 0.205 101 85 -115 10.3 102 85-115 10.2 96.9 85 -115 9.7 92.0 85 -155 0.18 Batch: BWDI 105 Date Analyzed: 04/27/2022 92.7 85 -115 9.5 99.2 85 -115 0.198 98.0 85-115 10.0 98.8 85 -115 9.9 93.8 85-115 9.4 88.2 85 -155 0.18 Batch: BWE0724 Date Analyzed: 05/16/2022 91 .7 85 -155 0.18 Matrix Spike -EPA 200. 7 Batch: BWD1104 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/26/2022 86.9 70 -130 59.1 50.2 85.7 70 -130 0.171 ND 95.5 70 -130 22.7 13.0 99.3 70 -130 12.5 2.6 91.0 70 -130 23.2 14.1 90.0 70 -130 0.18 ND SpkValue MRL OF 0.2 1.00 0.03 1.00 0.2 1.00 0.5 1.00 0.5 1.00 0.10 1.00 0.2 1.00 0.03 1.00 0.2 1.00 0.5 1.00 0.5 1.00 0.10 1.00 0.10 1.00 10.2 0.2 1.00 0.200 0.02 1.00 10.2 0.2 1.00 10.0 0.5 1.00 10.0 0.5 1.00 0.200 0.02 1.00 10.2 0.2 1.00 0.200 0.02 1.00 10.2 0.2 1.00 10.0 0.5 1.00 10.0 0.5 1.00 0.200 0.02 1.00 0.200 0.02 1.00 10.2 0.2 1.00 0.200 0.02 1.00 10.2 0.2 1.00 10.0 0.5 1.00 10.0 0.5 1.00 0.200 0.02 1.00 QC Report for Work Order (WO) -22D1197 Analyte % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL Matrix Spike -EPA 200.7 (cont.) QC Sample ID: BWDl I04-MS2 Batch: BWD1104 QC Source Sample: 22Dl 197-01 Date Prepared: 04/26/2022 Date Analyzed: 04/27/2022 Calcium, Dissolved 50.6 70 -130 356 351 10.2 0.2 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Iron, Dissolved 92.0 70 -130 0.184 ND 0.200 0.02 Magnesium, Dissolved 83.7 70 -130 186 177 10.2 0.2 Potassium, Dissolved 101 70-130 17.6 7.6 10.0 0.5 Sodium, Dissolved 80.1 70-130 125 117 10.0 0.5 Tin, Dissolved 87.2 70 -130 0.19 0.01 0.200 0.02 QC Sample ID: BWD1105-MS1 Batch: BWD1105 QC Source Sample: 22D 1197-11 Date Prepared: 04/26/2022 Date Analyzed: 04/27/2022 Calcium, Dissolved 92.6 70-130 424 415 10.2 0.2 Iron, Dissolved 109 70 -130 1.30 1.09 0.200 0.02 Magnesium, Dissolved 105 70 -130 213 202 10.2 0.2 Potassium, Dissolved 96.5 70 -130 25.3 15.7 10.0 0.5 Sodium , Dissolved 85.0 70 -130 404 395 10.0 0.5 Tin, Dissolved 90.0 70 -130 0.19 0.008 0.200 0.02 QC Sample ID: BWE0724-MS1 Batch: BWE0724 QC Source Sample: XXXXXXX-XX Date Prepared: 05/16/2022 Date Analyzed: 05/16/2022 Tin, Dissolved 102 70-130 0.20 0.002 0.200 0.02 Matrix Spike Dup -EPA 200.7 QC Sample ID: BWDl 104-MSDl Batch: BWD1104 QC Source Sample: XXXXXXX-XX Date Prepared: 04/26/2022 Date Analyzed: 04/26/2022 Calcium, Dissolved 85.5 0.246 70-130 20 58.9 50.2 10.2 0.2 Iron, Dissolved 85.7 0.00 70 -130 20 0.171 ND 0.200 0.02 Magnesium, Dissolved 98.6 1.38 70 -130 20 23.0 13.0 10.2 0.2 Potassium, Dissolved 103 3.01 70 -130 20 12.9 2.6 10.0 0.5 Sodium, Dissolved 93.8 1.21 70 -130 20 23.5 14.1 10.0 0.5 Tin, Dissolved 94.6 4.88 70 -130 20 0.19 ND 0.200 0.02 QC Sample ID: BWD1104-MSD2 Batch: BWD1104 QC Source Sample: 22Dll97-0l Date Prepared: 04/26/2022 Date Analyzed: 04/27/2022 Calcium, Dissolved 40.9 0.278 70 -130 20 355 351 10.2 0.2 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Iron, Dissolved 94.8 3.00 70 -130 20 0.190 ND 0.200 0.02 Magnesium, Dissolved 81.1 0.143 70 -130 20 185 177 10.2 0.2 Potassium, Dissolved 102 0.484 70 -130 20 17.7 7.6 10.0 0.5 Sodium, Dissolved 78.7 0.104 70 -130 20 125 117 10.0 0.5 Tin, Dissolved 86.9 0.268 70 -130 20 0.19 0.01 0.200 0.02 QC Sample ID: BWDl 105-MSDl Batch: BWDI 105 QC Source Sample: 22Dll97-11 Date Prepared: 04/26/2022 Date Analyzed: 04/27/2022 Calcium, Dissolved 58.6 0.820 70 -130 20 421 415 10.2 0.2 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Iron, Dissolved 105 0.577 70 -130 20 1.30 1.09 0.200 0.02 Magnesium, Dissolved 99.1 0.261 70 -130 20 212 202 10.2 0.2 Potassium, Dissolved 96.7 0.0853 70 -130 20 25.3 15.7 10.0 0.5 CtF WO#: 22D1197 www.ChemtechFord.com OF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 Analyte QC Sample ID: BWDI 105-MSDI Date Prepared: 04/26/2022 Sodium, Dissolved Tin, Dissolved QC Sample ID: BWE0724-MSD1 Date Prepared: 05/16/2022 Tin, Dissolved CtF WO#: 22D1197 www.ChemtechFord.com QC Report for Work Order (WO) -22D1197 %Rec RPD Limits RPD Max Result Source Cone Matrix Spike Dup -EPA 200.7 (cont.) Batch: BWD1105 QC Source Sample: 22Dll97-11 Date Analyzed: 04/27/2022 94.2 0.228 70-130 20 405 395 91.4 1.48 70 -130 20 0.19 0.008 Batch: BWE0724 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/16/2022 102 0.197 70 -130 20 0.20 0.002 Spk Value MRL DF 10.0 0.5 1.00 0.200 0.02 1.00 0.200 0.02 1.00 QC Report for Work Order (WO) -2201197 Analyte %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 200.8 QC Sample ID: BWD1080-BLK1 Batch: BWD1080 Date Prepared: 04/26/2022 Date Analyzed: 04/26/2022 Arsenic, Dissolved ND 0.0050 1.00 Beryllium, Dissolved ND 0.0005 1.00 Cadmium, Dissolved ND 0.0005 1.00 Chromium, Dissolved ND 0.0250 1.00 Cobalt, Dissolved ND 0.010 1.00 Copper, Dissolved ND 0.0100 1.00 Lead, Dissolved ND 0.0010 1.00 Manganese, Dissolved ND 0.0100 1.00 Molybdenum, Dissolved ND 0.0100 1.00 Nickel, Dissolved ND 0.0200 1.00 Selenium, Dissolved ND 0.0050 1.00 Silver, Dissolved ND 0.010 1.00 Thallium, Dissolved ND 0.0002 1.00 Uranium, Dissolved ND 0.0003 1.00 Vanadium, Dissolved ND 0.0150 1.00 Zinc, Dissolved ND 0.01 1.00 LCS -EPA 200.8 QC Sample ID: BWD1080-BSI Batch: BWD1080 Date Prepared: 04/26/2022 Date Analyzed: 04/26/2022 Arsenic, Dissolved 93.8 85 -115 0.038 0.0400 0.0005 1.00 Beryllium, Dissolved 94.0 85 -115 0.038 0.0400 0.0005 1.00 Cadmium, Dissolved 95.0 85 -115 0.038 0.0400 0.0002 1.00 Chromium, Dissolved 97.4 85 -115 0.039 0.0400 0.0005 1.00 Cobalt, Dissolved 97.7 85 -115 0.039 0.0400 0.0005 1.00 Copper, Dissolved 94.3 85 -115 0.038 0.0400 0.0010 1.00 Lead, Dissolved 104 85 -115 0.041 0.0400 0.0005 1.00 Manganese, Dissolved 101 85 -115 0.040 0.0400 0.0005 1.00 Molybdenum, Dissolved 98.8 85 -115 0.040 0.0400 0.0005 1.00 Nickel, Dissolved 93.4 85 -115 0.0373 0.0400 0.0005 1.00 Selenium, Dissolved 97.4 85 -115 0.039 0.0400 0.0005 1.00 Silver, Dissolved 98.7 85 -115 0.039 0.0400 0.0005 1.00 Thallium, Dissolved 108 85 -115 0.043 0.0400 0.0002 1.00 Uranium, Dissolved 103 85 -115 0.041 0.0400 0.0003 1.00 Vanadium, Dissolved 98.0 85-115 0.039 0.0400 0.0005 1.00 Zinc, Dissolved 94.1 85 -115 0.04 0.0400 0.01 1.00 Matrix Spike -EPA 200.8 QC Sample ID: BWD1080-MSI Batch: BWD1080 QC Source Sample: 22DI I 97-01 Date Prepared: 04/26/2022 Date Analyzed: 04/26/2022 Arsenic, Dissolved 98.2 70 -130 0.039 ND 0.0400 0.0005 1.00 Beryllium, Dissolved 96.7 70 -130 0.039 ND 0.0400 0.0005 1.00 Cadmium, Dissolved 89.3 70 -130 0.036 0.00005 0.0400 0.0002 1.00 Chromium, Dissolved 92.3 70 -130 0.038 0.0008 0.0400 0.0005 1.00 Cobalt, Dissolved 89.3 70 -130 0.036 0.0007 0.0400 0.0005 1.00 Copper, Dissolved 82.3 70 -130 0.034 0.001 0.0400 0.0010 1.00 Lead, Dissolved 92.3 70 -130 0.037 ND 0.0400 0.0005 1.00 Manganese, Dissolved 94.3 70 -130 0.038 0.0003 0.0400 0.0005 1.00 Molybdenum, Dissolved 103 70 -130 0.045 0.003 0.0400 0.0005 1.00 Nickel, Dissolved 83.1 75 -125 0.0368 0.0035 0.0400 0.0005 1.00 Selenium, Dissolved 98.1 70 -130 0.138 0.099 0.0400 0.0005 1.00 Silver, Dissolved 93.1 70 -130 0.037 ND 0.0400 0.0005 1.00 CtF WO#: 22D1197 www.ChemtechFord.com QC Report for Work Order (WO) -2201197 Analyte % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL Matrix Spike -EPA 200.8 (cont.) QC Sample ID: BWDI080-MS1 Batch: BWDI080 QC Source Sample: 22DI197-0l Date Prepared: 04/26/2022 Date Analyzed: 04/26/2022 Thallium, Dissolved 98.2 70-130 0.040 0.0002 0.0400 0.0002 Uranium, Dissolved 93.8 70 -130 0.060 0.022 0.0400 0.0003 Vanadium, Dissolved 96.8 70-130 0.039 0.0003 0.0400 0.0005 Zinc, Dissolved 81.3 70 -130 0.03 0.0007 0.0400 0.01 QC Sample ID: BWD1080-MS2 Batch: BWDI 080 QC Source Sample: 22DI197-ll Date Prepared: 04/26/2022 Date Analyzed: 04/26/2022 Arsenic, Dissolved 96.4 70 -130 0.043 0.004 0.0400 0.0005 Beryllium, Dissolved 96.4 70 -130 0.039 ND 0.0400 0.0005 Cadmium, Dissolved 87.7 70 -130 0.035 0.00003 0.0400 0.0002 Chromium, Dissolved 89.7 70 -130 0.038 0.002 0.0400 0.0005 Cobalt, Dissolved 85.4 70 -130 0.038 0.004 0.0400 0.0005 Copper, Dissolved 80.0 70 -130 0.034 0.002 0.0400 0.0010 Lead, Dissolved 90.6 70 -130 0.036 ND 0.0400 0.0005 Manganese, Dissolved 290 70 -130 5.13 5.02 0.0400 0.0025 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Molybdenum, Dissolved Nickel, Dissolved Selenium, Dissolved Silver, Dissolved Thallium, Dissolved Uranium, Dissolved Vanadium, Dissolved Zinc, Dissolved CtF WO#: 22D1197 www.ChemtechFord.com 102 79.2 110 86.8 96.5 91.2 94.7 81.0 70 -130 0.043 0.002 0.0400 75 -125 0.0376 0.0059 0.0400 70 -130 0.046 0.002 0.0400 70 -130 0.035 ND 0.0400 70 -130 0.039 0.0002 0.0400 70 -130 0.052 0.015 0.0400 70 -130 0.038 0.0005 0.0400 70 -130 0.04 0.008 0.0400 0.0005 0.0005 0.0005 0.0005 0.0002 0.0003 0.0005 0.01 OF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 5.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 Analyte QC Sample ID: BWD1038-BLK1 Date Prepared: 04/25/2022 Mercury, Dissolved QC Sample ID: BWD1038-BS1 Date Prepared: 04/25/2022 Mercury, Dissolved QC Sample ID: BWD1038-MS1 Date Prepared: 04/25/2022 Mercury, Dissolved QC Sample ID: BWD1038-MS2 Date Prepared: 04/25/2022 Mercury, Dissolved QC Sample ID: BWD1038-MSD1 Date Prepared: 04/25/2022 Mercury, Dissolved QC Sample ID: BWDI038-MSD2 Date Prepared: 04/25/2022 Mercury, Dissolved CtF WO#: 22D1197 www.ChemtechFord.com QC Report for Work Order (WO) -22D1197 %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 245.1 Batch: BWD1038 Date Analyzed: 04/26/2022 ND 0.0005 1.00 LCS -EPA 245.1 Batch: BWD1038 Date Analyzed: 04/26/2022 111 85 -115 0.0055 0.00500 0.0002 1.00 Matrix Spike -EPA 245.1 Batch: BWD1038 QC Source Sample: 22Dl 197-01 Date Analyzed: 04/26/2022 107 75 -125 0.0054 ND 0.00500 0.0002 1.00 Batch: BWD1038 QC Source Sample: 22Dll97-02 Date Analyzed: 04/26/2022 110 75 -125 0.0055 ND 0.00500 0.0002 1.00 Matrix Spike Dup -EPA 245.1 Batch: BWDI038 QC Source Sample: 22Dl197-0l Date Analyzed: 04/26/2022 112 4.76 75 -125 20 0.0056 ND 0.00500 0.0002 1.00 Batch: BWDI038 QC Source Sample: 22D1197-02 Date Analyzed: 04/26/2022 119 7.55 75 -125 20 0.0059 ND 0.00500 0.0002 1.00 QC Report for Work Order (WO) -22D1197 Analyte %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 300.0 QC Sample ID: BWD0707-BLKI Batch: BWD0707 Date Prepared: 04/18/2022 Date Analyzed: 04/18/2022 Chloride ND 1.0 1.00 Fluoride ND 0.1 1.00 Sulfate ND 1.0 1.00 QC Sample ID: BWD0714-BLK1 Batch: BWD0714 Date Prepared: 04/19/2022 Date Analyzed: 04/19/2022 Chloride ND 1.0 1.00 Fluoride ND 0.1 1.00 Sulfate ND 1.0 1.00 QC Sample ID: BWEOI41-BLK1 Batch: BWE0141 Date Prepared: 05/04/2022 Date Analyzed: 05/04/2022 Fluoride ND 0.1 1.00 LCS -EPA 300.0 QC Sample ID: BWD0707-BS1 Batch: BWD0707 Date Prepared: 04/18/2022 Date Analyzed: 04/18/2022 Chloride 96.0 90 -110 48.0 50.0 1.0 1.00 Fluoride 93.6 90 -110 4.7 5.00 0.1 1.00 Sulfate 94.1 90 -110 47.1 50.0 1.0 1.00 QC Sample ID: BWD0714-BS1 Batch: BWD0714 Date Prepared: 04/19/2022 Date Analyzed: 04/19/2022 Chloride 95.6 90 -110 47.8 50.0 1.0 1.00 Fluoride 96.1 90 -110 4.8 5.00 0.1 1.00 Sulfate 93.7 90 -110 46.9 50.0 1.0 1.00 QC Sample ID: BWE0141-BS1 Batch: BWE0141 Date Prepared: 05/04/2022 Date Analyzed: 05/04/2022 Fluoride 108 90 -110 5.4 5.00 0.1 1.00 Matrix Spike -EPA 300.0 QC Sample ID: BWD0707-MS1 Batch: BWD0707 QC Source Sample: XXXXXXX-XX Date Prepared: 04/18/2022 Date Analyzed: 04/18/2022 Chloride 102 80 -120 29.0 17.6 11.1 1.1 1.00 Fluoride 101 80 -120 2.1 0.9 1.11 0.1 1.00 Sulfate 98.7 80 -120 22.5 11 .5 11.1 1.1 1.00 QC Sample ID: BWD0707-MS2 Batch: BWD0707 QC Source Sample: 22D1197-01 Date Prepared: 04/19/2022 Date Analyzed: 04/19/2022 Chloride 95.3 80 -120 563 372 200 22.0 1.00 Fluoride 85.6 80 -120 17.6 0.5 20.0 2.2 1.00 Sulfate 93.7 80 -120 1370 1180 200 22.0 1.00 QC Sample ID: BWD0714-MS1 Batch: BWD07I4 QC Source Sample: 22Dll97-03 Date Prepared: 04/19/2022 Date Analyzed: 04/19/2022 Chloride 86.9 80 -120 440 5.8 500 55.0 1.00 Fluoride 83.2 80 -120 41.6 ND 50.0 5.5 1.00 Sulfate 94.0 80 -120 2390 1920 500 55.0 1.00 QC Sample ID: BWD0714-MS2 Batch: BWD0714 QC Source Sample: 22D1197-04 Date Prepared: 04/19/2022 Date Analyzed: 04/19/2022 Chloride 90.7 80 -120 487 33.4 500 55.0 1.00 Fluoride 88.1 80 -120 44.0 ND 50.0 5.5 1.00 Sulfate 89.6 80 -120 2040 1590 500 55.0 1.00 CtF WO#: 22D1197 www.ChemtechFord.com QC Report for Work Order (WO) -22D1197 Analyte %Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Matrix Spike -EPA 300.0 (cont.) QC Sample ID: BWE0141-MS1 Batch: BWE0141 QC Source Sample: XXXXXXX-XX Date Prepared: 05/04/2022 Date Analyzed: 05/04/2022 Fluoride 52.3 80 -120 63.0 10.8 100 11.0 1.00 QM-RPD -The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPD. QC Sample ID: BWEOI41-MS2 Batch: BWEOI41 QC Source Sample: XXXXXXX-XX Date Prepared: 05/04/2022 Date Analyzed: 05/04/2022 Fluoride 102 80 -120 22.1 1.8 20.0 2.2 Matrix Spike Dup -EPA 300.0 QC Sample ID: BWD0707-MSD1 Batch: BWD0707 QC Source Sample: XXXXXXX-XX Date Prepared: 04/18/2022 Date Analyzed: 04/18/2022 Chloride 101 0.671 80 -120 20 28.8 17.6 11.1 1.1 Fluoride 99.2 0.876 80 -120 20 2.0 0.9 1.11 0.1 Sulfate 96.7 0.983 80 -120 20 22.3 11.5 11.1 1.1 QC Sample ID: BWD0707-MSD2 Batch: BWD0707 QC Source Sample: 22Dll97-0l Date Prepared: 04/19/2022 Date Analyzed: 04/19/2022 Chloride 96.8 0.552 80 -120 20 566 372 200 22.0 Fluoride 85.4 0.200 80 -120 20 17.6 0.5 20.0 2.2 Sulfate 100 0.949 80 -120 20 1380 1180 200 22.0 QC Sample ID: BWD0714-MSD1 Batch: BWD0714 QC Source Sample: 22Dll97-03 Date Prepared: 04/19/2022 Date Analyzed: 04/19/2022 Chloride 90.3 3.72 80 -120 20 457 5.8 500 55.0 Fluoride 87.0 4.52 80 -120 20 43.5 ND 50.0 5.5 Sulfate 91 .7 0.476 80 -120 20 2380 1920 500 55.0 QC Sample ID: BWD0714-MSD2 Batch: BWD0714 QC Source Sample: 22Dll97-04 Date Prepared: 04/19/2022 Date Analyzed: 04/19/2022 Chloride 96.3 5.55 80 -120 20 515 33.4 500 55.0 Fluoride 90.9 3.15 80 -120 20 45.5 ND 50.0 5.5 Sulfate 102 2.97 80 -120 20 2100 1590 500 55.0 QC Sample ID: BWE0141-MSD1 Batch: BWEOI41 QC Source Sample: XXXXXXX-XX Date Prepared: 05/04/2022 Date Analyzed: 05/04/2022 Fluoride 64.2 17.4 80 -120 20 75.0 10.8 100 11 .0 QM-RPD -The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPD. QC Sample ID: BWEOI41-MSD2 Date Prepared: 05/04/2022 Fluoride CtF WO#: 22D1197 www.ChemtechFord.com Batch: BWE014I QC Source Sample: XXXXXXX-XX Date Analyzed: 05/04/2022 101 0.199 80-120 20 22.0 1.8 20.0 2.2 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 Analyte QC Sample ID : BWD1032-BLK1 Date Prepared: 04/25/2022 Ammonia as N QC Sample ID: BWE0243-BLK1 Date Prepared: 05/05/2022 Ammonia as N QC Sample ID: BWD1032-BS1 Date Prepared: 04/25/2022 Ammonia as N QC Sample ID: BWE0243-BSI Date Prepared: 05/05/2022 Ammonia as N QC Sample ID: BWD1032-MS1 Date Prepared: 04/25/2022 Ammonia as N QC Sample ID: BWE0243-MS I Date Prepared: 05/05/2022 Ammonia as N QC Sample ID: BWE0243-MS2 Date Prepared: 05/05/2022 Ammonia as N QC Sample ID: BWD1032-MSD1 Date Prepared: 04/25/2022 Ammonia as N QC Sample ID: BWE0243-MSD1 Date Prepared: 05/05/2022 Ammonia as N QC Sample ID: BWE0243-MSD2 Date Prepared: 05/05/2022 Ammonia as N CtF WO#: 22D1197 www.ChemtechFord.com QC Report for Work Order (WO) -22D1197 % Rec RPD Limits RPD Max Result Source Cone Blank -EPA 350.1 Batch: BWD1032 Date Analyzed: 04/25/2022 ND Batch: BWE0243 Date Analyzed: 05/05/2022 ND LCS -EPA 350.1 Batch: BWD1032 Date Analyzed: 04/25/2022 93.4 90 -110 4.67 Batch: BWE0243 Date Analyzed: 05/05/2022 92.7 90 -110 0.93 Matrix Spike -EPA 350.1 Batch: BWD1032 QC Source Sample: 2201197-01 Date Analyzed: 04/25/2022 103 80 -120 5.14 ND Batch: BWE0243 QC Source Sample: 22Dl 197-01 Date Analyzed: 05/05/2022 83.6 80 -120 0.84 ND Batch: BWE0243 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/05/2022 95.2 80 -120 1.18 0.23 Matrix Spike Dup -EPA 350.1 Batch: BWD1032 QC Source Sample: 22Dl197-0l Date Analyzed: 04/25/2022 100 2.56 80 -120 20 5.01 ND Batch: BWE0243 QC Source Sample: 22Dl 197-0 I Date Analyzed: 05/05/2022 92.2 9.77 80 -120 20 0.92 ND Batch: BWE0243 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/05/2022 91 .3 3.38 80 -120 20 1.14 0.23 SpkValue MRL DF 0.2 1.00 0.05 1.00 5.00 0.2 1.00 1.00 0.05 1.00 5.00 0.2 1.00 1.00 0.05 1.00 1.00 0.05 1.00 5.00 0.2 1.00 1.00 0.05 1.00 1.00 0.05 1.00 QC Report for Work Order (WO) -22D1197 Analyte % Rec RPO Limits RPO Max Result Source Cone SpkValue Blank -EPA 353.2 QC Sample ID: BWD0885-BLK1 Batch: BWD0885 Date Prepared: 04/21/2022 Date Analyzed: 04/21/2022 Nitrate + Nitrite, Total, as N ND LCS -EPA 353.2 QC Sample ID: BWD0885-BS 1 Batch: BWD0885 Date Prepared: 04/21/2022 Date Analyzed: 04/21/2022 Nitrate + Nitrite, Total, as N 103 80 -120 2.1 2.00 Matrix Spike -EPA 353.2 QC Sample ID: BWD0885-MS1 Batch: BWD0885 QC Source Sample: XXXXXXX-XX Date Prepared: 04/21/2022 Date Analyzed: 04/21/2022 Nitrate + Nitrite, Total, as N 111 80 -120 2.8 1.7 1.00 QC Sample ID: BWD0885-MS2 Batch: BWD0885 QC Source Sample: 22Dll97-0l Date Prepared: 04/21/2022 Date Analyzed: 04/21/2022 Nitrate+ Nitrite, Total, as N 78.1 80 -120 18 18 1.00 \ QM-010 -The MS recovery was outside acceptance limits but passed Duplicate Spike acceptance limits. The batch was accepted based on the acceptability of the MSD as the batch Spike. QC Sample ID: BWD0885-MSD1 Date Prepared: 04/21/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWD0885-MSD2 Date Prepared: 04/21/2022 Nitrate + Nitrite, Total, as N CtF WO#: 22D1197 www.ChemtechFord.com Matrix Spike Dup -EPA 353.2 Batch: BWD0885 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/21/2022 98.1 4.69 80 -120 20 2.7 1.7 Batch: BWD0885 QC Source Sample: 22Dll97-0l Date Analyzed: 04/21/2022 109 1.66 80 -120 20 19 18 1.00 1.00 MRL OF 0.1 1.00 0.1 1.00 0.1 1.00 0.5 5.00 0.1 1.00 0.5 5.00 QC Report for Work Order (WO) -2201197 Analyte %Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -EPA 82600 /5030A QC Sample ID: BWD1078-BLK1 Batch: BWD1078 Date Prepared: 04/25/2022 Date Analyzed: 04/25/2022 Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 J-.LOW -Estimated low due to low recovery of LCS or CCV Chloroform ND 1.0 1.00 J-LOW -Estimated low due to low recovery of LCS or CCV Chloromethane ND 1.0 1.00 J-LOW -Estimated low due to low recovery of LCS or CCV Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 LCS -EPA 82600 /5030A QC Sample ID: BWD1078-BSI Batch: BWD1078 Date Prepared: 04/25/2022 Date Analyzed: 04/25/2022 Acetone 82.0 70 -130 82.0 100 10.0 1.00 Benzene 81.9 70 -130 8.19 10.0 1.0 1.00 Carbon Tetrachloride 73.2 70 -130 7.32 10.0 1.0 1.00 J-LOW -Estimated low due to low recovery of LCS or CCV Chloroform 78.8 70 -130 7.88 10.0 1.0 1.00 J-LOW -Estimated low due to low recovery of LCS or CCV Chloromethane 71.9 70 -130 7.19 10.0 1.0 1.00 J-LOW -Estimated low due to low recovery of LCS or CCV Methyl Ethyl Ketone 97.2 70 -130 97.2 100 10.0 1.00 Methylene Chloride 86.0 70 -130 8.60 10.0 1.0 1.00 Naphthalene 89.6 70 -130 8.96 10.0 1.0 1.00 Tetrahydrofuran 101 70 -130 10.1 10.0 1.0 1.00 Toluene 81 .2 70 -130 8.12 10.0 1.0 1.00 Xylenes, total 84.7 70 -130 25.4 30.0 1.0 1.00 Matrix Spike -EPA 82600 /5030A QC Sample ID: BWD1078-MS1 Batch: BWD1078 QC Source Sample: 22Dll97-01 Date Prepared: 04/25/2022 Date Analyzed: 04/25/2022 Acetone 94.1 70 -130 94.1 ND 100 10.0 1.00 Benzene 112 70 -130 11 .2 ND 10.0 1.0 1.00 Carbon Tetrachloride 115 70 -130 11 .5 ND 10.0 1.0 1.00 J-LOW -Estimated low due to low recovery of LCS or CCV Chloroform 108 70 -130 10.8 ND 10.0 1.0 1.00 J-LOW -Estimated low due to low recovery of LCS or CCV Chloromethane 73.2 70 -130 7.32 ND 10.0 1.0 1.00 J-LOW -Estimated low due to low recovery of LCS or CCV Methyl Ethyl Ketone 112 70 -130 112 ND 100 10.0 1.00 Methylene Chloride 114 70 -130 11.4 ND 10.0 1.0 1.00 Naphthalene 112 70 -130 11.2 ND 10.0 1.0 1.00 Tetrahydrofuran 133 70 -130 13.3 ND 10.0 1.0 1.00 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. Toluene 114 70 -130 11.4 ND 10.0 1.0 1.00 CtF WO#: 22D1197 www.ChemtechFord.com QC Report for Work Order (WO) -2201197 Analyte % Rec RPD Limits RPD Max Result Source Cone Matrix Spike -EPA 8260D /5030A (cont.) QC Sample ID: BWDI078-MSI Batch: BWD1078 QC Source Sample: 22DI197-0l Date Prepared: 04/25/2022 Date Analyzed: 04/25/2022 Xylenes, total 117 70 -130 35.1 Matrix Spike Oup -EPA 82600 /5030A QC Sample ID: BWD1078-MSDI Batch: BWD1078 QC Source Sample: 22DII97-01 Date Prepared: 04/25/2022 Date Analyzed: 04/25/2022 Acetone 88.7 5.92 70 -130 20 88.7 Benzene 98.4 13.3 70 -130 20 9.84 Carbon Tetrachloride 98.7 15.1 70 -130 20 9.87 J-LOW -Estimated low due to low recovery of LCS or CCV Chloroform 95.3 12.3 J-LOW -Estimated low due to low recovery of LCS or CCV Chloromethane 84.3 14.1 J-LOW -Estimated low due to low recovery of LCS or CCV Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total CtF WO#: 22D1197 www.ChemtechFord.com 102 8.48 98.8 14.0 97.9 13.4 118 12.1 96.8 16.3 104 12.2 70 -130 20 9.53 70 -130 20 8.43 70 -130 20 102 70 -130 20 9.88 70 -130 20 9.79 70 -130 20 11.8 70 -130 20 9.68 70 -130 20 31.0 ND ND ND ND ND ND ND ND ND ND ND ND SpkValue MRL DF 30.0 1.0 1.00 100 10.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 100 10.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 30.0 1.0 1.00 Analyte QC Sample ID: BWD0681-BLK1 Date Prepared: 04/16/2022 Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) QC Sample ID: BWD0682-BLKI Date Prepared: 04/16/2022 Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) QC Sample ID: BWD0681-DUPI Date Prepared: 04/16/2022 Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Alkalinity -Total (as CaC03) QC Sample ID: BWD0681-DUP2 Date Prepared: 04/16/2022 Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Alkalinity -Total (as CaC03) QC Sample ID: BWD0682-DUP1 Date Prepared: 04/16/2022 Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Alkalinity -Total (as CaC03) QC Sample ID: BWD0681-BS1 Date Prepared: 04/16/2022 Alkalinity -Total (as CaC03) QC Sample ID: BWD0682-BS1 Date Prepared: 04/16/2022 Alkalinity -Total (as CaC03) CtF WO#: 22D1197 www.ChemtechFord.com QC Report for Work Order (WO) -22D1197 %Rec RPO Limits RPO Max Result Source Cone Blank -SM 2320 B Batch: B WD068 J Date Analyzed: 04/16/2022 ND ND Batch: B WD0682 Date Analyzed: 04/16/2022 ND ND Duplicate -SM 2320 B Batch: BWD0681 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/16/2022 0.498 20 220 222 20 ND ND 0.498 20 220 222 Batch: BWD0681 QC Source Sample: 22Dll97-0l Date Analyzed: 04/16/2022 8.96 20 180 164 20 ND ND 8.96 20 180 164 Batch: BWD0682 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/1 6/2022 1.15 20 360 355 20 ND ND 1.15 20 360 355 LCS -SM 2320 B Batch: BWD0681 Date Analyzed: 04/16/2022 99.1 90 -110 234 Batch: BWD0682 Date Analyzed: 04/16/2022 99.1 90 -110 234 SpkValue MRL OF 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 236 1.0 1.00 236 1.0 1.00 Analyte QC Sample ID: BWD0693-BLKI Date Prepared: 04/18/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD0700-BLK1 Date Prepared: 04/18/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD0752-BLK1 Date Prepared: 04/19/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD0693-DUP1 Date Prepared: 04/18/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD0693-DUP2 Date Prepared: 04/18/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD0700-DUP1 Date Prepared: 04/18/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD0700-DUP2 Date Prepared: 04/18/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD0752-DUP1 Date Prepared: 04/19/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD0752-DUP2 Date Prepared: 04/19/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD0693-BS1 Date Prepared: 04/18/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD0700-BS1 Date Prepared: 04/18/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD0752-BS1 Date Prepared: 04/19/2022 Total Dissolved Solids (TDS) CtF WO#: 22D1197 www.ChemtechFord.com QC Report for Work Order (WO) -2201197 %Rec RPD Limits RPD Max Result Source Cone SpkValue MRL DF Blank -SM 2540 C Batch: BWD0693 Date Analyzed: 04/18/2022 ND 10 1.00 Batch: BWD0700 Date Analyzed: 04/18/2022 ND 10 1.00 Batch: BWD0752 Date Analyzed: 04/19/2022 ND 10 1.00 Duplicate -SM 2540 C Batch: BWD0693 QC Source Sample: 22DI 197-01 Date Analyzed: 04/18/2022 5 10 4500 4300 500 1.00 Batch: BWD0693 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/18/2022 2 10 460 470 50 1.00 Batch: BWD0700 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/18/2022 10 10 528 480 20 1.00 Batch: BWD0700 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/18/2022 4 10 496 476 20 1.00 Batch: BWD0752 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/19/2022 0 10 690 690 50 1.00 Batch: BWD0752 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/19/2022 3 10 440 428 20 1.00 LCS -SM 2540 C Batch: BWD0693 Date Analyzed: 04/18/2022 102 90 -110 408 400 20 1.00 Batch: BWD0700 Date Analyzed: 04/18/2022 100 90 -110 400 400 20 1.00 Batch: BWD0752 Date Analyzed: 04/19/2022 100 90 -110 400 400 20 1.00 Surrogates Report for Work Order (WO) -22D1197 QCID Analyte BWD1078-BLK1 1,2-Dichloroethane-d4 BWD1078-BLK1 4-Bromofluorobenzene BW01078-BLK1 Toluene-dB BWD1078-BS1 1,2-Dichloroethane-d4 BWD1078-BS1 4-Bromofluorobenzene BWD1078-BS1 Toluene-dB BWD1078-MS1 1,2-Dichloroethane-d4 BWD1078-MS1 4-Bromofluorobenzene BWD1078-MS1 Toluene-dB BWD1078-MSD1 1,2-Dichloroethane-d4 BWD1078-MSD1 4-Bromofluorobenzene BWD1078-MSD1 Toluene-dB CtF WO#: 2201197 www.ChemtechFord.com %Rec LCL UCL Result Blank -EPA 8260D /5030A 97.9 64.2 126 9.79 99.4 71.4 122 9.94 100 63.2 129 10.0 LCS -EPA 8260D /5030A 96.5 64.2 126 9.65 102 71.4 122 10.2 98.3 63.2 129 9.83 Matrix Spike -EPA 8260D /5030A 94.1 64.2 126 9.41 101 71 .4 122 10.1 98.9 63.2 129 9.89 Matrix Spike Dup -EPA 8260D /5030A 94.5 64.2 126 9.45 101 71.4 122 10.1 98.5 63.2 129 9.85 Spk Value Batch OF 10.0 BWD1078 1.00 10.0 BWD1078 1.00 10.0 BW01078 1.00 10.0 BW01078 1.00 10.0 BW01078 1.00 10.0 BW01078 1.00 10.0 BW01078 1.00 10.0 BW01078 1.00 10.0 BW01078 1.00 10.0 BW01078 1.00 10.0 BWD1078 1.00 10.0 BWD1078 1.00 Surrogate Recoveries (Field Samples) LabNumber Analyte 8260 Low Level Volatiles 2201197-01 4-Bromofluorobenzene 2201197-01 Toluene-d8 2201197-01 1,2-0ichloroethane-d4 8260 Low Level Volatiles 2201197-02 1,2-0ichloroethane-d4 2201197-02 2201197-02 4-Bromofluorobenzene Toluene-d8 8260 Low Level Volatiles 2201197-03 Toluene-d8 2201197-03 2201197-03 1,2-0ichloroethane-d4 4-Bromofluorobenzene 8260 Low Level Volatiles 2201197-04 Toluene-d8 2201197-04 2201197-04 1,2-0ichloroethane-d4 4-Bromofluorobenzene 8260 Low Level Volatiles 2201197-05 1,2-0ichloroethane-d4 2201197-05 2201197-05 4-Bromofluorobenzene Toluene-d8 8260 Low Level Volatiles 2201197-06 4-Bromofluorobenzene 2201197-06 2201197-06 1,2-Dichloroethane-d4 Toluene-d8 8260 Low Level Volatiles 2201197-07 4-Bromofluorobenzene 2201197-07 2201197-07 Toluene-d8 1,2-0ichloroethane-d4 8260 Low Level Volatiles 2201197-08 1,2-0ichloroethane-d4 2201197-08 4-Bromofluorobenzene CtF WO#: 2201197 www.ChemtechFord.com Result 10.1 9.84 9.13 9.94 10.0 9.92 9.62 9.99 9.55 9.98 9.52 9.83 9.53 9.91 9.78 9.76 9.89 9.98 9.86 10.0 9.64 9.81 9.91 SpkLvl 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 %Rec 101 98.4 91.3 99.4 100 99.2 96 .2 99.9 95.5 99.8 95.2 98 .3 95.3 99.1 97.8 97.6 98.9 99.8 98.6 100 96.4 98.1 99.1 LCL UCL Qualifier 71 .4 122 63.2 129 64.2 126 64.2 126 71.4 122 63.2 129 63.2 129 64.2 126 71.4 122 63.2 129 64.2 126 71.4 122 64.2 126 71 .4 122 63.2 129 71.4 122 64.2 126 63.2 129 71.4 122 63.2 129 64.2 126 64.2 126 71.4 122 22D1197-08 Toluene-dB 8260 Low Level Volatiles 2201197-09 Toluene-dB 22D1197-09 22D1197-09 1,2-Dichloroethane-d4 4-Bromofluorobenzene 8260 Low Level Volatiles 22D1197-1 O Toluene-dB 22D1197-10 22D1197-10 1,2-Dichloroethane-d4 4-Bromofluorobenzene 8260 Low Level Volatiles 22D1197-11 1,2-Dichloroethane-d4 22D1197-11 22D1197-11 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22D1197-12 Toluene-dB 22D1197-12 22D1197-12 1,2-Dichloroethane-d4 4-Bromofluorobenzene CtF WO#: 22D1197 www.ChemtechFord.com 10.0 10.0 9.86 9.84 9.88 9.86 9.76 9.60 9.80 9.94 10.0 9.87 9.82 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 100 100 98.6 98.4 98.8 98.6 97.6 96.0 98.0 99.4 100 98.7 98.2 63.2 129 63.2 129 64.2 126 71.4 122 63.2 129 64.2 126 71.4 122 64.2 126 71.4 122 63.2 129 63.2 129 64.2 126 71.4 122 9632 South 500 West CHEMTECH·FORD LA60RI\TORIES 6/2/2022 Work Order: 22D 1691 Pro.ject: 2nd Quarter Cround Water 2022 Energy Fuels Resources, Inc. Attn: Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Client Service Contact: 801.262.7299 The analyses presented on this report were performed in accordance with the National Environmental Laboratory Accreditation Program (NELAP) unless noted in the comments, flags, or case narrative. If the report is to be used for regulatory compliance, it should be presented in its entirety, and not be altered. Approved By: Melissa Connolly, Project Manager Sandy, Utah 84070 801.262.7299 Main 866.792.0093 Fax Serving the lntermountain West since 1953 www.ChemtechFord.com CHEMTECH-FORD LABOAATORIES Energy Fuels Resources, Inc. Project: 2nd Quarter Ground Water 2022 Project Manager: Tanner Holliday Laboratory ID 2201691-01 22D1691-02 2201691-03 2201691-04 22D1691-05 2201691-06 2201691-07 22D1691-08 22D1691-09 22D1691-10 2201691-11 22D1691-12 22D1691-13 2201691-14 Sample Name MW-05 _ 04182022 MW-11 _04182022 MW-14_04182022 MW-17 _04182022 MW-12_04192022 MW-15_04192022 MW-28_04192022 MW-40_04192022 MW-26_04202022 MW-30 _ 04202022 MW-39 _ 04202022 MW-36_04212022 MW-70_04212022 Trip Blank Work Order Report Narrative Set Comments Due to laboratory error during the 82600 analysis, the LCS, MS, and MSD were not spiked for Tetrahydrofuran. The samples were analyzed for spectral evidence of Tetrahydrofuran . Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions The corrective action required with this workorder is to implement a new procedure to verify which analytes need to be spiked if they are not included in the laboratory standard spiking solution. Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 2201691 I CHEMTECH·FORD 1.A90AAfQlllltj Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Certificate of Analysis Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations ND= Not detected at the corresponding Minimum Reporting Limit (MRL). PO#: Receipt: 4/22/22 13:30@ 0.9 ·c Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 I mg/L = one milligram per liter or 1 mg/kg= one milligram per kilogram = I part per million I ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram= 1 part per billion. I ng/L = one nanogram per liter or I ng/kg = one nanogram per kilogram = 1 part per trillion Flag Descriptions A-01 = The sample was analyzed for spectral evidence ofTHF and none was detected. A-0 la = This analyte has been evaluated and reported to the MDL of 0.1 mg/L Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 22D1691 Page 30 of50 American West Analytical Laboratories 463 W. 3600 S. Sall Lake City, lJT 84115 Phone# (801) 263-8686 Toll Free# (888) 26;;..a586 L~ Fax# (801) 263-8687 Email awal@awaHabs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: Email: tholllda:,@aamufuela.com; KWelllel@eneqyfaela.com Project Name: 2nd Quarter Ground Water 2022 Project#: PO#: Sampler Name: Tanner Holliday I IIW-05 04182022 I IIW-11_04182022 1 IIW-14_04182~ I IIW-l 7 _04182022 , IIW-12_04192022 3 4 5 6 ; IIW-15_04192022 ' IIW-28_04192022 8 1 IIW-40_04192022 9 • KW-26 04202022 ll llW-30_04202022 I IIW-39_04202022 :!. IIW-36_04212022 Sample ID: R~ by._::) ~ ~~ / ~natin 1---;-..=., .... , ,.. _.· JC u """'Name: Tamo<Hol"""" ~by. -- """"Name: RelinqulSlte!l by: Slanature """'Name; Relinqlbhl!<I by: l!san- IPmtName: Date Samoled 4/18/2022 4/18/2022 4/18/2022 4/18/2022 4/19/2022 4/19/2022 4/19/2022 4/19/2022 4/20/2022 4/20/2022 4/20/2022 4/21/2022 ate; <(!21n<IZ ""'"' 11N Onttt nme: Date: 111me: Dale: rnme: Time Sampled 1500 1120 1SOO 1155 925 104S 1445 13SO 1400 1140 1100 740 Received by: SiQnal\.-e """'Name; CHAIN OF CUSTODY All analysis win be conducted using NElAP -m-and all data wi" be n,ported using AWAL's s1andard analyle lists and reporting limits (Pat.) unless speciflcally requested otherwise on this Chain of Custody and/or attached docunentalion. QC Level: Tum Around Time: Unless other arrangements have been made, signed repor1s will be emailed by 5:00 pm on 3 Standard the day lhey ""' due. x Include EDD: 0 LOCUS UPLOAD :E OI u EXCEL 00 00 X Field Filtered For: :r: --:E Dtasolved lletala ~ s:: 1/) :E :i .... C'I t <G ~ z For Compliance With: c i s:: D NELAP C) N D RCRA \ c' C'I :i > D CWA c ~ C) \ c u ::i D SOWA --"' 0 1 ... iii' C) D ELAP/A2LA ~ .. ~ u ~-0 C) r/J D NLLAP c-l' C) ~ -! .. -D Non-Compliance "' C) u ~ ~ .. II) Q .. D Other: 0 ~ • 'C 00 Q' I!! l:2. g Q' j • u < .. C) .. )( \i C) I> \() C :s 8 5l .... i ,; ,; § C'I "iii .. II) Ill r/J ~ c' ~ II'; ~ ['cf ~ 'i Known Hazards 0 .!! ..... ..... r,j z IQ i u "' 2 e \ a, ~ : < & 'o E \ . ~ :a II .. ·.: u Q ! Samole Comments .. V) 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X Date: Special Instructions: '"""' 2 i !)/(. r I AWAL Lab Sample Set# Page of I"··"·" Laboraloly Use Only iSampleoWfft: 1 Shipped or hand delivered 2 Ambient or Chllled 3 Tamperaue 4 Received Bmlcorll.eakJng (Improperly 5ealed) y N 5 Properly Preserved y N Checked at bench y N 6 Received Within HoklngTimes y N ~QC Tape Waa: 1 Present on Otm Pacl<age y N NA 2 Unbroken on OJler Package y N NA 3 Present on Sample y N NA 4 UnblDken on Sample y N NA -Sample ~ and COC Reconl? y N Sample containers for metals were field filtered. See the 2 "C Rec,ilvud ~ e o(J '__/ ~ vi.---..._ . J / .,,, h .. I_-,__ Analytical Scope of Work for Reporting Limits and VOC analyte """'Name"'? ft1,u; .. -J+... /, ', -, '"""' f t,?.,. i\ list. __/ Received by: I I uau,: ls1anaiure ,rne: IPmtName: !Received by: Date: lsianature rnme: IPnn1 Name: I American West Analytical Laboratories 463 W. 3600 S. Salt Lake City, UT 84115 Phone# (801) 263-8686 Ton Free# (688) 263-8686 L~ Fax # (801) 263-8687 Email awal@awal-labs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 S. Rwy. 191 Blanding, UT 84511 Contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: Email: tboll.lda,€eucrr:,fti.elll.com; KWehlel@eneqyfa.ela.com Project Name: 2nd Quarter Ground Water 2022 Project#: PO#: Sampler Name: Ta-er Holliday Date Samole ID: Samoled 1 IIW-70 04212022 4/21/2022 'Trip Blank ; I I 28 I I ! 2 22 I I ,~-by: ...::J,.J!lll" Y://_ ./. -v ""-Name: Tamer Holl"'-I Re!lnqushed by: "''"nature PrinlName: !Relinquished by: l!:lnna11n Print Name: IRelinqushed by: """- ICMMName; 4/18/2022 Date: 4/21 1rrne: 11"" !Dale: mme: Dale: 111me: Date: 1rrue: CHAIN OF CUSTODY Z":z 1 I (c 9 / All analy.,is will be conducted using NELAP accredl1ed methods and an data will be reported using AWAL's S1andard analyte lists and reporting llmHs (POL) unless speclflcally requested olherwise on lhis Chain of Cuslody and/or attached documenlallon. AWAL Lab Sample Set# Paga 2 of 2 I QC Level: I Tum Around Time: Unless o1her ana,gements have _, made. l°'•D•~ signed reports will be emailed by 5:00 pm on 3 Standard lhe day lhey are due. )< Include EDD: Laboratory Use Only 0 LOCUB UPLOAD ::.: "' u EXCEL ~plesWem: 00 00 X Field Filtered For: --;i:: ::.: DlaolYed Metala ..... cl' 1 Shipped or hand delivered It) ::.: :,i 'I-<Ii" 2 Ambient or et-.ec, C'I J:J-~ p.. z For Compliance With: 0 ,; c D NELAP 3 Temperatun, ·c c::, rz. N D RCRA o' C'I :,;-> D CWA ' Received BIDl<en/1.oaklng ci r::-C) 0 C) :5 D SOWA (Improperly 5ealed) --<'l 0 D ELAP/A2LA ..... ixi" c::, y N 0 ... ~ () c-I) D NLLAP l/) c::, r/) ~ c::, C'I -! ..: D Non-l::ompliance 5 Prope,1yPreserved <'l c::, "J C) ~ ::i ... It) £:!. ... D Other: y N I) ~ • "ti G' (2. c:, G' '5 • () "° • Checkedatbench ~ < C) >( c::, ... c::, Cl IO y N C :s C') c::, li 'I-ii 1 ,; ,; 5 C'I s m i It) l/) ID r/) ~ 6 RecelvedWill'in C ::!, ~ ~ .!: .. Known Hazards 0 .. ..... a ..... 0 ,,; :i 1111 • Holding Timas Time u a. s i ll '5 • < u & 0 E &: ~ • II g y N Samoled .. iS 0 Samole Comments .. en II; u .. 740 7 w X X X X X X X X X X 1120 3 w X COC Tape Was: 1 Prasenl on outer Paclcage y N NA 2 Unbroken on Outer Package y N NA 3 -onSemple y N NA 4 !Jmroken on Semple y N NA k)locrepandes Belween Semple ~ -COC Record? y N ~ecetved by: Date: Special Instructions: ,me: Print Name: Sample containers for metals were field filtered. See the Recl!lved..!>D-• t fl. c-lJ., / o"'J /z :u{ "L-Analytical Scope of Work for Reporting Limits and voe analyte --.1 ., -..Name: .f..J,1 ~Y. t "Tlme: /">;;, list. 3-i, Received by: , ( Date: Slonatun, Time: Print Name: Received by: Dale: Slonature Time: PrintName: I Work Order # 2 1.. ~ I Cc 9 / Delivery Method: ~UPS D USPS o reeltx D cnemtecn Louner D Walk-in D Customer Courier ; .. !Z )'ff~vyc"'j_rc,-, . 0,. 'e .,.. 1 r-( '.,, f 'i J Y ~?' 1_ " :c ! 1 / j 0 Chernted'I Lot II > LI b " or jJ ~ .. Sample# Container Preservative E .. ; ::c 0/-n r; J'YJ ,~_,Ji 'e J. /v' ,, I 1 1 ., I- 4 _/,' /-le., }. 1 rJ"/,1 ,-, I/~ f- V\J ,.7) I , .;l .,, . I I ., - r} It/ lJ c~J c/1'.:. I- ~ i LI I "' " 5 -~ > .D .. "O "' ,; .£ I.: ~ .£ C: ..., .. f f l!i "' Misc Volume (oz/ml) CHEMTECH FORD LABORATORIES Sample Receipt Receiving Temperature C'-7 ·c Comments - CHEMTECH-FORD L ,.~ 8. 0 P. r, T c:· R 1 t: S Sample Condition ( check If yes ) \ Containers Intact CO( can be matched to bottles Received on Ice Headspace Present (VO() Temperature Blank D Received within Holding Time Plastic Containers A· Plastic Unpreserved B-Miscellaneous Plastic C· Cyanide Qt (NaOH) E-Coliform/Ecoli/HPC F-Sulfide Qt (Zn Acetate) l-Mercury 1631 M Metal,;, Pint (HN03J N-Nutrient Pini (H2S04) R Radiolo~1cal IHN03) S· Sludge Cups/Tubs Q-Plastic Bag Glass Containers D-6251Na2S20ll G-Glass Unpreserved H-HAAS (NH4CIJ J. 508/515/525 (Na2S03) 1(-515 3 Herbicides 0 Oil & Grease !HCIJ P Pr'lenols !H2SE>4) T-TOC/TOX IHlP04/ U· 531 [MCAA. Na2SI03J V-S24(THMs {Ascorbic Acid) w. B,Go voe 11:1 HCII X-Via! unoreservP.d Y f,]4/50.: 1Na2SZ03) I v.:~cr1'.,..-~ecus G1ass QC Report for Work Order (WO) -22D1691 Analyte %Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -EPA 200.7 QC Sample ID: BWE0047-BLK1 Batch: BWE0047 Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Calcium, Dissolved ND 0.2 1.00 Iron, Dissolved ND 0.03 1.00 Magnesium, Dissolved ND 0.2 1.00 Potassium, Dissolved ND 0.5 1.00 Sodium, Dissolved ND 0.5 1.00 Tin, Dissolved ND 0.10 1.00 QC Sample ID: BWE0048-BLK1 Batch: BWE0048 Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Calcium, Dissolved ND 0.2 1.00 Iron, Dissolved ND 0.03 1.00 Magnesium, Dissolved ND 0.2 1.00 Potassium, Dissolved ND 0.5 1.00 Sodium, Dissolved ND 0.5 1.00 Tin, Dissolved ND 0.10 1.00 LCS -EPA 200. 7 QC Sample ID: BWE0047-BS1 Batch: BWE0047 Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Calcium, Dissolved 94.0 85-115 9.6 10.2 0.2 1.00 Iron, Dissolved 101 85 -115 0.201 0.200 0.02 1.00 Magnesium, Dissolved 99.3 85 -115 10.1 10.2 0.2 1.00 Potassium, Dissolved 102 85 -115 10.2 10.0 0.5 1.00 Sodium, Dissolved 96.2 85 -115 9.6 10.0 0.5 1.00 Tin, Dissolved 92.3 85 -155 0.18 0.200 0.02 1.00 QC Sample ID: BWE0048-BS1 Batch: BWE0048 Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Calcium, Dissolved 96.2 85 -115 9.8 10.2 0.2 1.00 Iron, Dissolved 108 85 -115 0.216 0.200 0.02 1.00 Magnesium, Dissolved 102 85 -115 10.4 10.2 0.2 1.00 Potassium, Dissolved 105 85 -115 10.5 10.0 0.5 1.00 Sodium, Dissolved 98.7 85-115 9.9 10.0 0.5 1.00 Tin, Dissolved 92.8 85 -155 0.19 0.200 0.02 1.00 Matrix Spike -EPA 200.7 QC Sample ID: BWE0047-MS1 Batch: BWE0047 QC Source Sample: XXXXXXX-XX Date Prepared: 05/02/2022 Date Analyzed: 05 /02/2022 Calcium, Dissolved 88.8 70 -130 56.7 47.7 10.2 0.2 1.00 Iron, Dissolved 106 70-130 0.212 ND 0.200 0.02 1.00 Magnesium, Dissolved 98.4 70 -130 36.4 26.4 10.2 0.2 1.00 Potassium, Dissolved 104 70 -130 12.4 1.9 10.0 0.5 1.00 Sodium, Dissolved 89.4 70 -130 52.1 43.2 10.0 0.5 1.00 Tin, Dissolved 93.4 70 -130 0.19 0.003 0.200 0.02 1.00 QC Sample ID: BWE0047-MS2 Batch: BWE0047 QC Source Sample: XXXXXXX-XX Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Calcium, Dissolved 95.2 70 -130 36.9 27.2 10.2 0.2 1.00 Iron, Dissolved 106 70 -130 0.220 0.008 0.200 0.02 1.00 Magnesium, Dissolved 102 70-130 17.5 7.1 10.2 0.2 1.00 Potassium, Dissolved 107 70 -130 11 .7 1.0 10.0 0.5 1.00 Sodium, Dissolved 99.2 70-130 15.4 5.5 10.0 0.5 1.00 Tin, Dissolved 94.0 70 -130 0.19 0.004 0.200 0.02 1.00 CtF WO#: 2201691 www.ChemtechFord.com QC Report for Work Order (WO) -22D1691 Analyte %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL Matrix Spike -EPA 200.7 (cont.) QC Sample ID: BWE0048-MSI Batch: BWE0048 QC Source Sample: 22Dl691-0l Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Calcium, Dissolved 148 70 -130 134 119 10.2 0.2 QM-010 -The MS recovery was outside acceptance limits but passed Duplicate Spike acceptance limits. The batch was accepted based on the acceptability of the MSD as the batch Spike. Iron, Dissolved 107 70 -130 0.231 0.017 0.200 0.02 Magnesium, Dissolved 119 70 -130 48.3 36.1 10.2 0.2 Potassium, Dissolved 110 70 -130 18.0 7.0 10.0 0.5 Sodium, Dissolved -252 70 -130 433 458 10.0 0.5 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Tin, Dissolved 88.4 70 -130 0.19 0.009 0.200 0.02 Matrix Spike Dup-EPA 200.7 QC Sample ID: BWE0047-MSDI Batch: BWE0047 QC Source Sample: XXXXXXX-XX Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Calcium, Dissolved 91.8 0.544 70 -130 20 57.1 47.7 10.2 0.2 Iron, Dissolved 110 3.85 70 -130 20 0.220 ND 0.200 0.02 Magnesium, Dissolved 100 0.495 70 -130 20 36.6 26.4 10.2 0.2 Potassium, Dissolved 107 1.78 70 -130 20 12.6 1.9 10.0 0.5 Sodium, Dissolved 91.2 0.354 70 -130 20 52.3 43.2 10.0 0.5 Tin, Dissolved 95.6 2.29 70 -130 20 0.19 0.003 0.200 0.02 QC Sample ID: BWE0047-MSD2 Batch: BWE0047 QC Source Sample: XXXXXXX-XX Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Calcium, Dissolved 93.4 0.484 70 -130 20 36.7 27.2 10.2 0.2 Iron, Dissolved 106 0.136 70 -130 20 0.220 0.008 0.200 0.02 Magnesium, Dissolved 101 0.836 70 -130 20 17.3 7.1 10.2 0.2 Potassium, Dissolved 105 1.58 70 -130 20 11.5 1.0 10.0 0.5 Sodium, Dissolved 97.9 0.881 70-130 20 15.3 5.5 10.0 0.5 Tin, Dissolved 93.7 0.365 70 -130 20 0.19 0.004 0.200 0.02 QC Sample ID: BWE0048-MSDI Batch: BWE0048 QC Source Sample: 22Dl691-01 Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Calcium, Dissolved 76.6 5.57 70 -130 20 127 119 10.2 0.2 Iron, Dissolved 99.1 6.82 70 -130 20 0.215 0.017 0.200 0.02 Magnesium, Dissolved 92.1 5.93 70 -130 20 45.5 36.1 10.2 0.2 Potassium, Dissolved 99.9 5.86 70 -130 20 17.0 7.0 10.0 0.5 Sodium, Dissolved -493 5.73 70 -130 20 409 458 10.0 0.5 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Tin, Dissolved CtF WO#: 22D1691 www.ChemtechFord.com 88.9 0.591 70 -130 20 0.19 0.009 0.200 0.02 DF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 QC Report for Work Order (WO) -2201691 Analyte % Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Blank -EPA 200.8 QC Sample ID: BWE0023-BLK1 Batch: BWE0023 Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Arsenic, Dissolved ND 0.0050 1.00 Beryllium, Dissolved ND 0.0005 1.00 Cadmium, Dissolved ND 0.0005 1.00 Chromium, Dissolved ND 0.0250 1.00 Cobalt, Dissolved ND 0.010 1.00 Copper, Dissolved ND 0.0100 1.00 Lead, Dissolved ND 0.0010 1.00 Manganese, Dissolved ND 0.0100 1.00 Molybdenum, Dissolved ND 0.0100 1.00 Nickel, Dissolved ND 0.0200 1.00 Selenium, Dissolved ND 0.0050 1.00 Silver, Dissolved ND 0.010 1.00 Thallium, Dissolved ND 0.0002 1.00 Uranium, Dissolved ND 0.0003 1.00 Vanadium, Dissolved ND 0.0150 1.00 Zinc, Dissolved ND 0.01 1.00 QC Sample ID: BWE0816-BLK1 Batch: BWE0816 Date Prepared: 05/17/2022 Date Analyzed: 05/17/2022 Uranium, Dissolved ND 0.0003 1.00 LCS -EPA 200.8 QC Sample ID: BWE0023-BS1 Batch: BWE0023 Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Arsenic, Dissolved 95.6 85 -115 0.038 0.0400 0.0005 1.00 Beryllium, Dissolved 95.1 85 -115 0.038 0.0400 0.0005 1.00 Cadmium, Dissolved 97.7 85 -115 0.039 0.0400 0.0002 1.00 Chromium, Dissolved 98.2 85 -115 0.039 0.0400 0.0005 1.00 Cobalt, Dissolved 96.0 85 -115 0.038 0.0400 0.0005 1.00 Copper, Dissolved 92.7 85 -115 0.037 0.0400 0.0010 1.00 Lead, Dissolved 104 85 -115 0.041 0.0400 0.0005 1.00 Manganese, Dissolved 95.4 85 -115 0.038 0.0400 0.0005 1.00 Molybdenum, Dissolved 101 85 -115 0.040 0.0400 0.0005 1.00 Nickel, Dissolved 92.1 85 -115 0.0368 0.0400 0.0005 1.00 Selenium, Dissolved 97.2 85 -115 0.039 0.0400 0.0005 1.00 Silver, Dissolved 100 85 -115 0.040 0.0400 0.0005 1.00 Thallium, Dissolved 109 85 -115 0.044 0.0400 0.0002 1.00 Uranium, Dissolved 96.4 85 -115 0.039 0.0400 0.0003 1.00 Vanadium, Dissolved 96.1 85 -115 0.038 0.0400 0.0005 1.00 Zinc, Dissolved 93.5 85 -115 0.04 0.0400 0.01 1.00 QC Sample ID: BWE0816-BS1 Batch: BWE0816 Date Prepared: 05/17/2022 Date Analyzed: 05/17/2022 Uranium, Dissolved 99.5 85 -115 0.040 0.0400 0.0003 1.00 Matrix Spike -EPA 200.8 QC Sample ID: BWE0023-MS1 Batch: BWE0023 QC Source Sample: XXXXXXX-XX Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Arsenic, Dissolved 96.9 70 -130 0.039 0.0006 0.0400 0.0005 1.00 Beryllium, Dissolved 99.9 70 -130 0.040 ND 0.0400 0.0005 1.00 Cadmium, Dissolved 97.4 70 -130 0.039 ND 0.0400 0.0002 1.00 Chromium, Dissolved 97.4 70 -130 0.040 0.0009 0.0400 0.0005 1.00 Cobalt, Dissolved 95.9 70 -130 0.038 0.00009 0.0400 0.0005 1.00 CtF WO#: 2201691 www.ChemtechFord.com Analyte QC Sample ID: BWE0023-MS1 Date Prepared: 05/02/2022 Copper, Dissolved Lead, Dissolved Manganese, Dissolved Molybdenum, Dissolved Nickel, Dissolved Selenium, Dissolved Silver, Dissolved Thallium, Dissolved Uranium, Dissolved Vanadium, Dissolved Zinc, Dissolved QC Sample ID: BWE0816-MS1 Date Prepared: 05/17/2022 Uranium, Dissolved CtF WO#: 22D1691 www.ChemtechFord.com QC Report for Work Order (WO) -22D1691 %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Matrix Spike -EPA 200.8 (cont.) Batch: BWE0023 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/02/2022 89.4 70-130 0.036 0.0006 0.0400 0.0010 1.00 99.3 70 -130 0.040 ND 0.0400 0.0005 1.00 97.6 70 -130 0.039 0.0004 0.0400 0.0005 1.00 102 70 -130 0.041 0.0002 0.0400 0.0005 1.00 89.5 75 -125 0.0364 0.0006 0.0400 0.0005 1.00 99.6 70 -130 0.040 ND 0.0400 0.0005 1.00 99.0 70 -130 0.040 ND 0.0400 0.0005 1.00 108 70-130 0.043 ND 0.0400 0.0002 1.00 96.1 70 -130 0.039 0.0005 0.0400 0.0003 1.00 97.1 70 -130 0.040 0.0008 0.0400 0.0005 1.00 95.4 70 -130 0.04 ND 0.0400 0.01 1.00 Batch: BWE0816 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/17/2022 99.7 70 -130 1.99 ND 2.00 0.0150 1.00 Analyte QC Sample ID: BWEOOI8-BLKI Date Prepared: 05/02/2022 Mercury, Dissolved QC Sample ID: BWEOOI8-BSI Date Prepared: 05/02/2022 Mercury, Dissolved QC Sample ID: BWE0018-MSI Date Prepared: 05/02/2022 Mercury, Dissolved QC Sample ID: BWE0018-MS2 Date Prepared: 05/02/2022 Mercury, Dissolved QC Sample ID: BWE0018-MSD1 Date Prepared: 05/02/2022 Mercury, Dissolved QC Sample ID: BWEOOI8-MSD2 Date Prepared: 05/02/2022 Mercury, Dissolved CtF WO#: 2201691 www.ChemtechFord.com QC Report for Work Order (WO) -22D1691 % Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Blank -EPA 245.1 Batch: BWE0018 Date Analyzed: 05/03/2022 ND 0.0005 1.00 LCS -EPA 245.1 Batch: B WEOO 18 Date Analyzed: 05/03/2022 105 85 -115 0.0052 0.00500 0.0002 1.00 Matrix Spike -EPA 245.1 Batch: BWE0018 QC Source Sample: 22DI691-0l Date Analyzed: 05/03/2022 107 75 -125 0.0054 ND 0.00500 0.0002 1.00 Batch: BWEOOI8 QC Source Sample: 22Dl691-02 Date Analyzed: 05/03/2022 104 75 -125 0.0052 ND 0.00500 0.0002 1.00 Matrix Spike Dup -EPA 245.1 Batch: BWEOOI8 QC Source Sample: 22Dl691-01 Date Analyzed: 05/03/2022 104 3.61 75 -125 20 0.0052 ND 0.00500 0.0002 1.00 Batch: BWE0018 QC Source Sample: 22DI691-02 Date Analyzed: 05/03/2022 103 0.510 75 -125 20 0.0052 ND 0.00500 0.0002 1.00 QC Report for Work Order (WO) -22D1691 Analyte % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -EPA 300.0 QC Sample ID : BWDl 107-BLKl Batch: BWDl 107 Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Chloride ND 1.0 1.00 Fluoride ND 0.1 1.00 Sulfate ND 1.0 1.00 QC Sample ID: BWD1135-BLKl Batch: BWD1135 Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Chloride ND 1.0 1.00 Sulfate ND 1.0 1.00 QC Sample ID: BWE0043-BLK1 Batch: BWE0043 Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Chloride ND 1.0 1.00 Fluoride ND 0.1 1.00 Sulfate ND 1.0 1.00 QC Sample ID: BWE1087-BLK1 Batch: BWE1087 Date Prepared: 05/19/2022 Date Analyzed: 05/19/2022 Fluoride ND 0.1 1.00 LCS -EPA 300.0 QC Sample ID: BWD1107-BSl Batch: BWD1107 Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Chloride 95.7 90 -110 47.9 50.0 1.0 1.00 Fluoride 91 .0 90 -110 4.5 5.00 0.1 1.00 Sulfate 97.2 90 -110 48.6 50.0 1.0 1.00 QC Sample ID: BWD1135-BS1 Batch: BWD1135 Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Chloride 93.6 90 -110 46.8 50.0 1.0 1.00 Sulfate 95.5 90 -110 47.8 50.0 1.0 1.00 QC Sample ID: BWE0043-BS1 Batch: BWE0043 Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Chloride 93.8 90 -110 46.9 50.0 1.0 1.00 Fluoride 90.9 90 -110 4.5 5.00 0.1 1.00 Sulfate 93.5 90 -110 46.7 50.0 1.0 1.00 QC Sample ID: BWE1087-BS1 Batch: BWE1087 Date Prepared: 05/19/2022 Date Analyzed: 05/19/2022 Fluoride 103 90 -110 5.1 5.00 0.1 1.00 Matrix Spike -EPA 300.0 QC Sample ID: BWD1107-MSl Batch: BWD1107 QC Source Sample: 2201691-0l Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Chloride 95.4 80 -120 240 49.5 200 22.0 1.00 Fluoride 95.2 80 -120 19.8 0.8 20.0 2.2 1.00 Sulfate 107 80 -120 1360 1140 200 22.0 1.00 QC Sample ID: BWD1107-MS2 Batch: B WD1107 QC Source Sample: XXXXXXX-XX Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Chloride 97.0 80 -120 25.3 14.6 11 .1 1.1 1.00 Fluoride 94.8 80 -120 2.0 0.9 1.11 0.1 1.00 Sulfate 115 80 -120 28.1 15.3 11.1 1.1 1.00 QC Sample ID: BWD1135-MSI Batch: BWDI135 QC Source Sample: XXXXXXX-XX Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 CtF WO#: 22D1691 www.ChemtechFord.com QC Report for Work Order (WO) -2201691 Analyte %Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Matrix Spike -EPA 300.0 (cont.) QC Sample ID: BWDI 135-MSI Batch: BWDI 135 QC Source Sample: XXXXXXX-XX Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Chloride 94.2 80 -120 85.3 74.8 11.1 1.1 1.00 Sulfate 97.1 80 -120 70.9 60.1 11 .1 1.1 1.00 QC Sample ID: BWD1135-MS2 Batch: BWD1135 QC Source Sample: XXXXXXX-XX Date Prepared: 04/27/2022 DateAnalyzed: 04/27/2022 Chloride 91 .9 80 -120 108 16.3 100 11.0 1.00 Sulfate 91.1 80 -120 472 381 100 11 .0 1.00 QC Sample ID: BWE0043-MS1 Batch: BWE0043 QC Source Sample: 22D1691-02 Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Chloride 92.7 80 -120 522 58.5 500 55.0 1.00 Fluoride 89.9 80 -120 44.9 ND 50.0 5.5 1.00 Sulfate 71.5 80-120 1700 1340 500 55.0 1.00 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BWE0043-MS2 Batch: BWE0043 QC Source Sample: 22D1691-03 Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Chloride 95.2 80 -120 493 17.7 500 55.0 1.00 Fluoride 90.6 80 -120 45.3 ND 50.0 5.5 1.00 Sulfate 46.0 80 -120 2620 2390 500 55.0 1.00 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. I QC Sample ID: BWE1087-MSI Batch: BWE1087 QC Source Sample: XXXXXXX-XX Date Prepared: 05/19/2022 Date Analyzed: 05/19/2022 Fluoride 96.2 80 -120 4.8 ND 5.00 0.5 1.00 Matrix Spike Dup -EPA 300.0 QC Sample ID: BWD1107-MSD1 Batch: BWDl 107 QC Source Sample: 22Dl691-0l Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Chloride 89.0 5.47 80 -120 20 227 49.5 200 22.0 1.00 Fluoride 87.7 7.87 80 -120 20 18.3 0.8 20.0 2.2 1.00 Sulfate 99.0 1.19 80 -120 20 1340 1140 200 22.0 1.00 QC Sample ID: BWDl 107-MSD2 Batch: BWD1107 QC Source Sample: XXXXXXX-XX Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Chloride 99.2 0.980 80 -120 20 25.6 14.6 11 .1 1.1 1.00 Fluoride 99.1 2.43 80 -120 20 2.0 0.9 1.11 0.1 1.00 Sulfate 118 1.07 80 -120 20 28.4 15.3 11.1 1.1 1.00 QC Sample ID: BWD1l35-MSD1 Batch: BWD1135 QC Source Sample: XXXXXXX-XX Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Chloride 97.2 0.401 80 -120 20 85.6 74.8 11 .1 1.1 1.00 Sulfate 99.2 0.325 80 -120 20 71.1 60.1 11 .1 1.1 1.00 QC Sample ID: BWD1 l35-MSD2 Batch: BWDJ 135 QC Source Sample: XXXXXXX-XX Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Chloride 89.6 2.12 80 -120 20 106 16.3 100 11 .0 1.00 Sulfate 93.3 0.450 80 -120 20 474 381 100 11.0 1.00 QC Sample ID: BWE0043-MSD1 Batch: BWE0043 QC Source Sample: 22D1691-02 Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Chloride 94.0 1.30 80 -120 20 529 58.5 500 55.0 1.00 CtF WO#: 22D1691 www.ChemtechFord.com QC Report for Work Order (WO) -22D1691 Analyte %Rec RPD Limits RPD Max Result Source Cone SpkValue MRL Matrix Spike Dup -EPA 300.0 (cont.) QC Sample ID: BWE0043-MSD1 Batch: BWE0043 QC Source Sample: 22DI691-02 Date Prepared: 05/02/2022 Date Analyzed: 05/02/2022 Fluoride 91.7 1.99 80 -120 20 45.8 ND 50.0 5.5 Sulfate 62.3 2.76 80 -120 20 1650 1340 500 55.0 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BWE0043-MSD2 Batch: BWE0043 QC Source Sample: 22D1691-03 Date Prepared: 05/02/2022 Chloride Fluoride Sulfate Date Analyzed: 05/02/2022 94.3 0.836 80 -120 91 .4 0.894 80 -120 29.0 3.30 80 -120 20 20 20 489 45.7 2530 17.7 ND 2390 500 50.0 500 55.0 5.5 55.0 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BWEI087-MSD1 Date Prepared: 05/19/2022 Fluoride CtF WO#: 22D1691 www.ChemtechFord.com Batch: BWE1087 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/19/2022 96.3 0.0416 80 -120 20 4.8 ND 5.00 0.5 DF 1.00 1.00 1.00 1.00 1.00 1.00 Analyte QC Sample ID: BWD1276-BLK1 Date Prepared: 04/29/2022 Ammonia as N QC Sample ID: BWE0243-BLKI Date Prepared: 05/05/2022 Ammonia as N QC Sample ID: BWD1276-BSI Date Prepared: 04/29/2022 Ammonia as N QC Sample ID: BWE0243-BS1 Date Prepared: 05/05/2022 Ammonia as N QC Sample ID: BWD1276-MSI Date Prepared: 04/29/2022 Ammonia as N QC Sample ID: BWE0243-MS1 Date Prepared: 05/05/2022 Ammonia as N QC Sample ID: BWE0243-MS2 Date Prepared: 05/05/2022 Ammonia as N QC Sample ID: BWD1276-MSD1 Date Prepared: 04/29/2022 Ammonia as N QC Sample ID: BWE0243-MSD1 Date Prepared: 05/05/2022 Ammonia as N QC Sample ID: BWE0243-MSD2 Date Prepared: 05/05/2022 Ammonia as N CtF WO#: 22D1691 www.ChemtechFord.com QC Report for Work Order (WO) -22D1691 %Rec RPO Limits RPD Max Result Source Cone SpkValue MRL DF Blank -EPA 350.1 Batch: BWD1276 Date Analyzed: 05/03/2022 ND 0.2 1.00 Batch: BWE0243 Date Analyzed: 05/05/2022 ND 0.05 1.00 LCS -EPA 350.1 Batch: BWD1276 Date Analyzed: 05/03/2022 99.4 90 -110 4.97 5.00 0.2 1.00 Batch: BWE0243 Date Analyzed: 05/05/2022 92.7 90 -110 0.93 1.00 0.05 1.00 Matrix Spike -EPA 350.1 Batch: BWD1276 QC Source Sample: 22Dl691-0l Date Analyzed: 05/03/2022 102 80 -120 5.44 0.34 5.00 0.2 1.00 Batch: BWE0243 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/05/2022 83.6 80 -120 0.84 ND 1.00 0.05 1.00 Batch: BWE0243 QC Source Sample: 2201691-0l Date Analyzed: 05/05/2022 95.2 80 -120 1.18 0.23 1.00 0.05 1.00 Matrix Spike Dup -EPA 350.1 Batch: BWD1276 QC Source Sample: 22D 1691-01 Date Analyzed: 05/03/2022 98.1 3.64 80 -120 20 5.24 0.34 5.00 0.2 1.00 Batch: BWE0243 QC Source Sample: XX:XXXXX-XX Date Analyzed: 05/05/2022 92.2 9.77 80 -120 20 0.92 ND 1.00 0.05 1.00 Batch: BWE0243 QC Source Sample: 22Dl691-0l Date Analyzed: 05/05/2022 91 .3 3.38 80 -120 20 1.14 0.23 1.00 0.05 1.00 QC Report for Work Order (WO) -2201691 Analyte %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL QC Sample ID: BWDI022-BLKI Date Prepared: 04/25/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWDI022-BSI Date Prepared: 04/25/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWD1022-MSI Blank -EPA 353.2 Batch: BWD1022 Date Analyzed: 04/25/2022 ND LCS -EPA 353.2 Batch: BWD1022 Date Analyzed: 04/25/2022 108 80 -120 2.2 Matrix Spike -EPA 353.2 Batch: BWDI022 QC Source Sample: XXXXXXX-XX Date Prepared: 04/25/2022 Date Analyzed: 04/25/2022 2.00 Nitrate+ Nitrite, Total, as N 122 80 -120 4.9 3.6 1.00 0.1 0.1 0.2 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSO. The RPO between the MS and MSO was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO . QC Sample ID: BWD1022-MS2 Date Prepared: 04/25/2022 Nitrate+ Nitrite, Total, as N Batch: BWD1022 QC Source Sample: 22D169I-01 Date Analyzed: 04/25/2022 92.3 80 -120 1.2 Matrix Spike Dup -EPA 353.2 0.3 QC Sample ID: BWD1022-MSD1 Batch: BWDI022 QC Source Sample: XXXXXXX-XX Date Prepared: 04/25/2022 Date Analyzed: 04/25/2022 1.00 Nitrate+ Nitrite, Total, as N 121 0.227 80 -120 20 4.8 3.6 1.00 0.1 0.2 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSO. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BWD1022-MSD2 Date Prepared: 04/25/2022 Nitrate + Nitrite, Total, as N CtF WO#: 22D1691 www.ChemtechFord.com Batch: BWD1022 QC Source Sample: 22Dl691-0l Date Analyzed: 04/25/2022 102 8.21 80 -120 20 1.3 0.3 1.00 0.1 DF 1.00 1.00 2.00 1.00 2.00 1.00 QC Report for Work Order (WO) -22D1691 Analyte % Rec RPD Limits RPD Max Result Source Cone SpkValue MRL DF Blank -EPA 8260D /5030A QC Sample ID: BWD1117-BLKl Batch: B WD 1117 Date Prepared: 04/26/2022 Date Analyzed: 04/26/2022 Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 QC Sample ID: BWD1179-BLK1 Batch: BWD1179 Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 LCS -EPA 8260D /5030A QC Sample ID: BWD1117-BS1 Batch: BWDI 117 Date Prepared: 04/26/2022 Date Analyzed: 04/26/2022 Acetone 99.1 70 -130 99.1 100 10.0 1.00 Benzene 104 70 -130 10.4 10.0 1.0 1.00 Carbon Tetrachloride 113 70 -130 11.3 10.0 1.0 1.00 Chloroform 95.5 70 -130 9.55 10.0 1.0 1.00 Chloromethane 87.1 70 -130 8.71 10.0 1.0 1.00 Methyl Ethyl Ketone 110 70 -130 110 100 10.0 1.00 Methylene Chloride 108 70 -130 10.8 10.0 1.0 1.00 Naphthalene 100 70 -130 10.0 10.0 1.0 1.00 Tetrahydrofuran 70 -130 ND 10.0 1.0 1.00 Toluene 102 70-130 10.2 10.0 1.0 1.00 Xylenes, total 108 70 -130 32.4 30.0 1.0 1.00 QC Sample ID: BWDll 79-BSl Batch: BWD1179 Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Acetone 98.7 80 -120 98.7 100 10.0 1.00 Benzene 106 80 -120 10.6 10.0 1.0 1.00 Carbon Tetrachloride 108 80 -120 10.8 10.0 1.0 1.00 Chloroform 96.5 80 -120 9.65 10.0 1.0 1.00 Chloromethane 106 80 -120 10.6 10.0 1.0 1.00 Methyl Ethyl Ketone 108 80-120 108 100 10.0 1.00 Methylene Chloride 107 80 -120 10.7 10.0 1.0 1.00 Naphthalene 106 80 -120 10.6 10.0 1.0 1.00 Tetrahydrofuran 80 -120 ND 10.0 1.0 1.00 CtF WO#: 22D1691 www.ChemtechFord.com QC Report for Work Order (WO) -22D1691 Analyte %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF LCS -EPA 8260D /5030A (cont.) QC Sample ID: BWD1179-BSI Batch: BWD1179 Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Toluene 106 80 -120 10.6 10.0 1.0 1.00 Xylenes, total 109 80 -120 32.6 30.0 1.0 1.00 Matrix Spike -EPA 8260D /5030A QC Sample ID: BWDlll7-MSI Batch: BWDI ll 7 QC Source Sample: XXXXXXX-XX Date Prepared: 04/26/2022 Date Analyzed: 04/26/2022 Acetone 95.5 70 -130 477 500 50.0 1.00 Benzene 97.0 70 -130 48.5 50.0 5.0 1.00 Carbon Tetrachloride 100 70 -130 50.2 50.0 5.0 1.00 Chloroform 90.4 70 -130 45.2 50.0 5.0 1.00 Chloromethane 82.1 70 -130 41.0 50.0 5.0 1.00 Methyl Ethyl Ketone 96.8 70 -130 484 500 50.0 1.00 Methylene Chloride 97.9 70 -130 49.0 50.0 5.0 1.00 Naphthalene 94.0 70 -130 47.0 50.0 5.0 1.00 Tetrahydrofuran 70 -130 ND 50.0 5.0 1.00 Toluene 97.8 70 -130 48.9 50.0 5.0 1.00 Xylenes, total 100 70 -130 151 150 5.0 1.00 QC Sample ID: BWD1179-MSI Batch: BWD1179 QC Source Sample: 22Dl691-0l Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Acetone 86.7 70 -130 86.7 ND 100 10.0 1.00 Benzene 88.7 70 -130 8.87 ND 10.0 1.0 1.00 Carbon Tetrachloride 91.0 70 -130 9.10 ND 10.0 1.0 1.00 Chloroform 80.6 70 -130 8.06 ND 10.0 1.0 1.00 Chloromethane 89.1 70 -130 8.91 ND 10.0 1.0 1.00 Methyl Ethyl Ketone 90.4 70 -130 90.4 ND 100 10.0 1.00 Methylene Chloride 87.5 70 -130 8.75 ND 10.0 1.0 1.00 Naphthalene 91 .3 70 -130 9.13 ND 10.0 1.0 1.00 Tetrahydrofuran 70 -130 ND ND 10.0 1.0 1.00 Toluene 87.9 70 -130 8.79 ND 10.0 1.0 1.00 Xylenes, total 91.7 70 -130 27.5 ND 30.0 1.0 1.00 Matrix Spike Dup -EPA 8260D /5030A QC Sample ID: BWDI 117-MSDI Batch: BWD1117 QC Source Sample: XXXXXXX-XX Date Prepared: 04/26/2022 Date Analyzed: 04/26/2022 Acetone 98.9 3.47 70 -130 20 494 500 50.0 1.00 Benzene 98.0 1.03 70-130 20 49.0 50.0 5.0 1.00 Carbon Tetrachloride 97.0 3.35 70 -130 20 48.5 50.0 5.0 1.00 Chloroform 91 .6 1.32 70 -130 20 45.8 50.0 5.0 1.00 Chloromethane 85.3 3.82 70 -130 20 42.6 50.0 5.0 1.00 Methyl Ethyl Ketone 101 3.91 70 -130 20 503 500 50.0 1.00 Methylene Chloride 101 3.31 70 -130 20 50.6 50.0 5.0 1.00 Naphthalene 98.1 4.27 70 -130 20 49.0 50.0 5.0 1.00 Tetrahydrofuran 70 -130 20 ND 50.0 5.0 1.00 Toluene 96.7 1.13 70 -130 20 48.4 50.0 5.0 1.00 Xylenes, total 101 0.530 70 -130 20 151 150 5.0 1.00 QC Sample ID: BWDll 79-MSDI Batch: BWD1179 QC Source Sample: 22Dl691-0l Date Prepared: 04/27/2022 Date Analyzed: 04/27/2022 Acetone 87.4 0.896 70 -130 20 87.4 ND 100 10.0 1.00 Benzene 88.8 0.113 70 -130 20 8.88 ND 10.0 1.0 1.00 Carbon Tetrachloride 87.5 3.92 70-130 20 8.75 ND 10.0 1.0 1.00 Chloroform 82.4 2.21 70 -130 20 8.24 ND 10.0 1.0 1.00 CtF WO#: 2201691 www.ChemtechFord.com Analyte QC Sample ID: BWD1179-MSDI Date Prepared: 04/27/2022 Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total CtF WO#: 22D1691 www.ChemtechFord.com QC Report for Work Order (WO) -22D1691 %Rec RPD Limits RPDMax Result Source Cone Matrix Spike Dup -EPA 8260D /5030A (cont.) Batch: BWD1179 QC Source Sample: 22Dl691-0l Date Analyzed: 04/27/2022 93.6 4.93 70 -130 20 9.36 ND 96.2 6.17 70 -130 20 96.2 ND 90.3 3.15 70 -130 20 9.03 ND 88.1 3.57 70 -130 20 8.81 ND 70 -130 20 ND ND 88.4 0.567 70 -130 20 8.84 ND 91.3 0.473 70 -130 20 27.4 ND SpkValue MRL DF 10.0 1.0 1.00 100 10.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 30.0 1.0 1.00 Analyte QC Sample ID: BWDI003-BLK1 Date Prepared: 04/23/2022 Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) QC Sample ID: BWDI003-DUP1 Date Prepared: 04/23/2022 Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Alkalinity -Total (as CaC03) QC Sample ID: BWD1003-BS1 Date Prepared: 04/23/2022 Alkalinity -Total (as CaC03) CtF WO#: 22D1691 www.ChemtechFord.com QC Report for Work Order (WO) -2201691 %Rec RPD Limits RPD Max Result Source Cone SpkValue MRL DF Blank -SM 2320 B Batch: BWDI003 Date Analyzed: 04/23/2022 ND 1.0 1.00 ND 1.0 1.00 Duplicate -SM 2320 B Batch: BWDI003 QC Source Sample: 22Dl691-0l Date Analyzed: 04/23/2022 6.82 20 312 292 1.0 1.00 20 ND ND 1.0 1.00 6.82 20 312 292 1.0 1.00 LCS -SM 2320 B Batch: BWD1003 Date Analyzed: 04/23/2022 97.7 90 -110 231 236 1.0 1.00 Analyte QC Sample ID: BWDlOl 1-BLKl Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD1012-BLK1 Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD1013-BLK1 Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD1014-BLK1 Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWDlOll-DUPl Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD1011-DUP2 Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD10l2-DUP1 Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD1012-DUP2 Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD1013-DUP1 Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD1013-DUP2 Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD1014-DUP1 Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD1014-DUP2 Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD1011-BS1 Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD1012-BS1 Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) CtF WO#: 22D1691 www.ChemtechFord.com QC Report for Work Order (WO) -22D1691 % Rec RPD Limits RPDMax Result Source Cone Blank -SM 2540 C Batch: BWD1011 Date Analyzed: 04/25/2022 ND Batch: BWD1012 Date Analyzed: 04/25/2022 ND Batch: BWD1013 Date Analyzed: 04/25/2022 ND Batch: BWD1014 Date Analyzed: 04/25/2022 ND Duplicate -SM 2540 C Batch: BWDlOll QC Source Sample: 22D1691-01 Date Analyzed: 04/25/2022 8 10 1920 2080 Batch: BWD1011 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/25/2022 3 10 988 1020 Batch: BWD1012 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/25/2022 4 10 460 440 Batch: BWD1012 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/25/2022 10 ND 892 Batch: BWD1013 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/25/2022 4 10 928 964 Batch: BWD1013 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/25/2022 6 10 484 512 Batch: BWD1014 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/25/2022 8 10 924 996 Batch: BWD1014 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/25/2022 1 10 1720 1700 LCS -SM 2540 C Batch: BWD1011 Date Analyzed: 04/25/2022 96 90 -110 384 Batch: BWD1012 Date Analyzed: 04/25/2022 100 90 -110 400 SpkValue MRL DF 20 1.00 10 1.00 10 1.00 20 1.00 20 1.00 20 1.00 100 1.00 20 1.00 20 1.00 20 1.00 20 1.00 20 1.00 400 20 1.00 400 20 1.00 Analyte QC Sample ID: BWDI013-BSI Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) QC Sample ID: BWD1014-BSI Date Prepared: 04/25/2022 Total Dissolved Solids (TDS) CtF WO#: 22D1691 www.ChemtechFord.com QC Report for Work Order (WO) -22D1691 %Rec RPO Limits RPO Max Result LCS -SM 2540 C (cont.) Batch: BWD1013 Date Analyzed: 04/25/2022 99 90 -110 396 Batch: BWD1014 Date Analyzed: 04/25/2022 98 90 -110 392 Source Cone SpkValue MRL OF 400 20 1.00 400 20 1.00 Surrogates Report for Work Order (WO) -2201691 QCID Analyte BWD1117-BLK1 1,2-Dichloroethane-d4 BWD1117-BLK1 4-Bromofluorobenzene BWD1117-BLK1 Toluene-dB BWD1179-BLK1 1,2-Dichloroethane-d4 BWD1179-BLK1 4-Bromofluorobenzene BWD1179-BLK1 Toluene-dB BWD1117-BS1 1,2-Dichloroethane-d4 BWD1117-BS1 4-Bromofluorobenzene BWD1117-BS1 Toluene-dB BWD1179-BS1 1,2-Dichloroethane-d4 BWD1179-BS1 4-Bromofluorobenzene BWD1179-BS1 Toluene-dB BWD1117-MS1 1,2-Dichloroethane-d4 BWD1117-MS1 4-Bromofluorobenzene BWD1117-MS1 Toluene-dB BWD1179-MS1 1,2-Dichloroethane-d4 BWD1179-MS1 4-Bromofluorobenzene BWD1179-MS1 Toluene-dB BWD1117-MSD1 1,2-Dichloroethane-d4 BWD1117-MSD1 4-Bromofluorobenzene BWD1117-MSD1 Toluene-dB BWD1179-MSD1 1,2-Dichloroethane-d4 BWD1179-MSD1 4-Bromofluorobenzene BWD1179-MS01 Toluene-dB CtF WO#: 22D1691 www.ChemtechFord.com %Rec LCL UCL Result Blank -EPA 82600 /5030A 101 64.2 126 10.1 98.2 71.4 122 9.82 100 63.2 129 10.0 104 64.2 126 10.4 98.1 71.4 122 9.81 97.4 63.2 129 9.74 LCS -EPA 82600 /5030A 101 64.2 126 10.1 102 71.4 122 10.2 97.8 63.2 129 9.78 101 64.2 126 10.1 101 71.4 122 10.1 100 63.2 129 10.0 Matrix Spike -EPA 8260D /5030A 97.8 64.2 126 48.9 102 71.4 122 50.8 100 63.2 129 50.0 98.2 64.2 126 9.82 102 71.4 122 10.2 98.6 63.2 129 9.86 Matrix Spike Oup -EPA 82600 /5030A 98.0 64.2 126 49.0 99.1 71.4 122 49.6 100 63.2 129 50.0 96.6 64.2 126 9.66 100 71.4 122 10.0 99.6 63.2 129 9.96 SpkValue Batch DF 10.0 BWD1117 1.00 10.0 BWD1117 1.00 10.0 BWD1117 1.00 10.0 BWD1179 1.00 10.0 BWD1179 1.00 10.0 BWD1179 1.00 10.0 BWD1117 1.00 10.0 BWD1117 1.00 10.0 BWD1117 1.00 10.0 BWD1179 1.00 10.0 BWD1179 1.00 10.0 BWD1179 1.00 50.0 BWD1117 1.00 50.0 BWD1117 1.00 50.0 BWD1117 1.00 10.0 BWD1179 1.00 10.0 BWD1179 1.00 10.0 BWD1179 1.00 50.0 BWD1117 1.00 50.0 BWD1117 1.00 50.0 BWD1117 1.00 10.0 BWD1179 1.00 10.0 BWD1179 1.00 10.0 BWD1179 1.00 Surrogate Recoveries (Field Samples) LabNumber Analyte 8260 Low Level Volatiles 22D1691-01 4-Bromofluorobenzene 22D1691-01 Toluene-dB 22D1691-01 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22D1691-02 1,2-Dichloroethane-d4 22D1691-02 22D1691-02 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22D1691-03 1,2-Dichloroethane-d4 22D1691-03 22D1691-03 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22D1691-04 1,2-Dichloroethane-d4 22D1691-04 22D1691-04 4-Bromofluorobenzene · Toluene-dB 8260 Low Level Volatiles 22D1691-05 1,2-Dichloroethane-d4 22D1691-05 22D1691-05 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22D 1691-06 1,2-Dichloroethane-d4 22D1691-06 22D1691-06 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22D1691-07 4-Bromofluorobenzene 22D1691-07 22D1691-07 1,2-Dichloroethane-d4 Toluene-dB 8260 Low Level Volatiles 22D1691-08 4-Bromofluorobenzene 22D1691-08 Toluene-dB CtF WO#: 22D1691 www.ChemtechFord.com Result 10.0 9.87 10.0 10.1 9.64 10.0 10.1 9.67 9.89 10.0 9.74 10.0 10.6 9.64 10.0 10.8 9.81 9.81 9.66 10.5 9.95 9.97 10.0 SpkLvl 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 %Rec 100 98.7 100 101 96.4 100 101 96.7 98.9 100 97.4 100 106 96.4 100 108 98.1 98.1 96.6 105 99.5 99.7 100 LCL UCL Qualifier 71.4 122 63.2 129 64.2 126 64.2 126 71.4 122 63.2 129 64.2 126 71.4 122 63.2 129 64.2 126 71.4 122 63.2 129 64.2 126 71.4 122 63.2 129 64.2 126 71.4 122 63.2 129 71.4 122 64.2 126 63.2 129 71.4 122 63.2 129 22D1691-08 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22D1691-09 1,2-Dichloroethane-d4 2201691-09 22D1691-09 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22D1691-10 1,2-Dichloroethane-d4 22D1691-10 22D1691-10 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22D1691-11 1,2-Dichloroethane-d4 22D1691-11 22D1691-11 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22D1691 -12 1,2-Dichloroethane-d4 22D1691-12 22D1691-12 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22D1691-13 1,2-Dichloroethane-d4 22D1691-13 22D1691-13 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22D1691-14 Toluene-dB 22D1691-14 22D1691-14 1,2-Dichloroethane-d4 4-Bromofluorobenzene CtF WO#: 22D1691 www.ChemtechFord.com 10.7 10.4 9.83 10.0 9.98 9.75 10.0 10.3 10.2 9.87 10.2 9.64 10.0 10.1 9.95 9.94 10.0 10.3 9.71 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 107 104 98.3 100 99.8 97.5 100 103 102 98.7 102 96.4 100 101 99.5 99.4 100 103 97.1 64.2 126 64.2 126 71 .4 122 63.2 129 64.2 126 71.4 122 63.2 129 64.2 126 71.4 122 63.2 129 64.2 126 71.4 122 63.2 129 64.2 126 71.4 122 63.2 129 63.2 129 64.2 126 71.4 122 9632 South 500 \Nest CHEMTECH-FORD LA80RATORIES 6/2/2022 Work Order: 22D2139 Pro,ject: 2nd Quarter Ground Water 2022 Energy Fuels Resources, Inc. Attn: Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Client Service Contact: 801.262. 7299 The analyses presented on this report were performed in accordance with the National Environmental Laboratory Accreditation Program (NELAP) unless noted in the comments, flags, or case narrative. If the report is to be used for regulatory compliance, it should be presented in its entirety, and not be altered. Approved By: Melissa Connolly, Project Manager Sandy, Utah 84070 801.262.7299 Main 866.792.0093 Fax Serving the lntermountain West since 1953 www.ChemtechFord.com CHEMTECH-FORD LABO~.e..TOl!IE:S Energy Fuels Resources, Inc. Project: 2nd Quarter Ground Water 2022 Project Manager: Tanner Holliday Laboratory ID 2202139-01 2202139-02 2202139-03 2202139-04 2202139-05 2202139-06 2202139-07 2202139-08 Sample Name MW-22_04252022 MW-03A_04272022 MW-23_04272022 MW-24_ 04272022 MW-24A_04272022 MW-38_04272022 TW4-24_04272022 Trip Blank Work Order Report Narrative Set Comments Due to laboratory error during the 82600 analysis, the LCS, MS, and MSD were not spiked for Tetrahydrofuran. The samples were analyzed for spectral evidence of Tetrahydrofuran. Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions The corrective action required with this workorder is to implement a new procedure to verify which analytes need to be spiked if they are not included in the laboratory standard spiking solution. Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 2202139 CHEMTECH-FORD lA601P,T0RIES Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Certificate of Analysis Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations ND = Not detected at the corresponding Minimum Reporting Limit (MRL). PO#: Receipt: 4/29/22 11 :00@ 0.0 °C Date Reported: 6/2/2022 Project Name: 2nd Quarter Ground Water 2022 I mg/L = one milligram per liter or I mg/kg= one milligram per kilogram = I part per million. I ug/L = one microgram per liter or I ug/kg = one microgram per kilogram = l part per billion, I ng/L = one nanogram per liter or I ng/kg = one nanogram per kilogram = I part per trillion Flag Descriptions A-01 = The sample was analyzed for spectral evidence ofTHF and none was detected. Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 22D2139 Page 18 of 35 American West Analytical Laboratories 463 W. 3600 S. Salt Lake City, lJT 84115 Phone# (801) 263-8686 Toll Free# (688) 263-8686 1 Address: 6425 8. Hwy. 191 Blanding, UT 84511 Contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: Email: thoDhlaJ@ellerayfaela.com; KWeba~erufaela.com Project Name: 2nd Quarter Ground Water 2022 Project#: PO#: Sampler Name: Tanner Holliday IIW-22 04252022 I IIW--03A 04272022 (,'I (j2 (_\3 (\4 I IIW-23 04272022 1 IIW-24 04272022 i IIW-24A_04272022 1:! 5 ; IIW-38_04272022 .· .6 ,. ' TW4-24 04272022 I TRIPBLAIIK J 8 9 I C) I ;i SamolelD: Refinqub!Ed by: ) .. If. ./ ,/. L, ,~-• ' .. A'"-' --""'111 Name: Tanner........_ R~by: -... Prtn!Name: IRellnqulohedby: L-- ""'"'Name: Relinq,bhod by. ., ... _ Print Name: Date Samoled 4/25/2022 4/27/2022 4/27/2022 4/27/2022 4/27/2022 4/27/2022 4/27/2022 4/25/2022 Date: itme: 11M Date: nrne: uate: THTle: Oat,,: :nme: I Time Samoled 1250 915 840 800 740 1030 1230 1250 IReceMld by. - CHAIN OF CUSTODY AN anelysls will be cooducied using NElAP acaedlled m-and .. -will be reported using AW/U.'s ·-analyle lis1s and repom,g llmHB (POL) unless specfflcalty requested OlhelWise on this Chain of Custody anG'or attached documenlallon QC Level: I Tum Around Time: Unless other arrangements have been made, signed repor1s will be emaNed by 5:00 pm on 3 Standard Ille day !hey .... due, IX Include EDD: o' LOCUS UPLOAD ::. aS C) EXCEL 00 00 !x Foefd Rttered For: -:i:: ::. Dlaolved lletala ... r;: i.rj ::. ~ 'It' t'I t oi ~ z For Compliance With: c i. r;: D NELAP C N D RCRA o' t'I ;j >' D CWA c ;:::. C c C) ::i D SDWA -!") 0 D ELAP/A2LA ... ... ill C r;: c ~ C) 0 C rn D NLLAP c,j' lJ) C t'I -! ..: D Non-CompUance !") C !") (.) != l;i ... lJ) ~ ... D Other: 0 :t. • .,; 00 Q' ~ c:, Q' '5 II C) • e! < C .. X C • C II IO C: 5 (') C i 'It' " l .; .; -! t'I ~ .. 0 lJ) lJ) iii Cl rn ~ Known Hazards ls :. II: :t. ~ ,; .. -u -0 z 1111 • u a. N (') m 1 • < g & 0 E 0 ~ .;: i:! • II .. II: u i5 0 Samole Comments .. (J) ... 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 3 w X """': Special Instructions: ~e: 2-1,b-J,(;y AWAL Lab Sample Set# Page 1 of 1 I°"··· ... Laboratory Use Only !Samples Were: V ;/"') ,61-- 2 Amblenl ~ 3 TcmperallnJ C • G'C 4 Rec:eivecl Brol<ervloaklng empn,perty e 1 5 ~-N Ched<edatb<n;h y N 6-Wl1nln c:rThnes I N ICOCTapoWas: 1 ~ on Ouler Package Y . N NA 2 e-on Ouler Pacl<age Y N NA 3 PrMentonSample ~ y N 4 ~onsanpe ~ ~ Y N NA Belweal5anple ~yand coc A.econ!? c) CMH·Name: Sample containers for metals were field filtered. See the l\«:8"""b~.? /L D" ,t q /z.. l--/ Analytical Scope of Work for Reporting Limits and voe analyte --:_;,{,t L,~ r ~ k~ ~ ~ 0------/ IT!me//[·C, list. Prinl Nan~ ReceMldby: I Date: Sirmahfl' r,me: IPrinlName. !Received by: Date: '""'naue Time: Print Name: I 1-:Z: 9 Work Order# 2 2 t> .Z IJ '1 Delivery Method: UPS FedE D USPS Ch hC ouner Jurier 'Lf?~ &7{ff Chemtedi Lot# DI' Sample# Container Preservative G t -c i' ;; L C: (t'e._.1 t-l 1/ c If'., __ f ~;i, c!t~~;f d ,. If ,. l---I/; r- r , ?-) ~'\..) \_: C '/II ''<.__ I- :: ci E l a: 'a .! E ~ ~ ::. I ~ v ~ l 5 ;;- I j tl 1 0 ~ .it ¥ s Ii: l s "' ; -~ ;;-"' Misc Volume Cor/mlj CHEMTECH FORD LABORATORIES Sample Receipt Receiving Temperature C, c.· ·c - Comments CHEMTECH-FORD I.A60 R ... '\TQ.~1ES Sample Condition (check if yes J COC can be matched to bottles Sufficent Sample Volume Received within Holding Time Plastic Containers P.· Plastic unpreserved 8-Miscellaneous Plastic C-Cyan;de Qt (NaOH) E· Coliform/Ecoti/HPC F-Sulfide Qt (Zn Acetate) L· Mercury 1631 M-Metals Pint IHN03) N-Nutrient Pint (H2SOA) R-Radiolog;cal (HN03) S-Sludge Cups/Tubs Q-Plastic Bag Glass Containers D-625 (Na2S203) G-Glass Unpreserved H-HAAS (NHQCI) I-508/515/525 (Na2S03) IC-S1SL3 Herbicides 0-0il & Grease (HCI} P-Phenols (H2S041 T-TOC/TOX (H3P041 U-531 (MCAA, Na2S203) V-524/THMs (Ascorbic Acid) W-8260 voe I U H(I) X-Vial Unpreserved V-624/504 (Na25203) Z Miscellaneous Glass QC Report for Work Order (WO) -22D2139 Analyte %Rec RPO limits RPO Max Result Source Cone Spk Value MRL Blank -EPA 200.7 QC Sample ID: BWE0432-BLK1 Batch: BWE0432 Date Prepared: 05/09/2022 Date Analyzed: 05/10/2022 Calcium, Dissolved ND 0.2 Iron, Dissolved ND 0.03 Magnesium, Dissolved ND 0.2 Potassium, Dissolved ND 0.5 Sodium, Dissolved ND 0.5 Tin , Dissolved ND 0.10 QC Sample ID: BWE0445-BLK1 Batch: BWE0445 Date Prepared: 05/10/2022 Date Analyzed: 05/10/2022 Calcium, Dissolved ND 0.2 Iron, Dissolved ND 0.03 Magnesium, Dissolved ND 0.2 Potassium, Dissolved ND 0.5 Sodium, Dissolved ND 0.5 Tin, Dissolved ND 0.10 LCS -EPA 200. 7 QC Sample ID: BWE0432-BS1 Batch: BWE0432 Date Prepared: 05 /09/2022 Date Analyzed: 05/10/2022 Calcium, Dissolved 85.4 85 -115 8.7 10.2 0.2 Iron, Dissolved 94.7 85-115 0.189 0.200 0.02 Magnesium, Dissolved 90.6 85-115 9.2 10.2 0.2 Potassium, Dissolved 92.2 85 -115 9.2 10.0 0.5 Sodium, Dissolved 95.0 85 -115 9.5 10.0 0.5 Tin, Dissolved 87.7 85 -155 0.18 0.200 0.02 QC Sample ID: BWE0445-BSl Batch: BWE0445 Date Prepared: 05/10/2022 Date Analyzed: 05 /11/2022 Calcium, Dissolved 93.3 85 -115 9.5 10.2 0.2 Iron, Dissolved 86.1 85 -115 0.172 0.200 0.02 Magnesium, Dissolved 86.7 85 -115 8.8 10.2 0.2 Potassium, Dissolved 87.6 85 -115 8.8 10.0 0.5 Sodium, Dissolved 99.3 85-115 9.9 10.0 0.5 Tin , Dissolved 98.2 85 -155 0.20 0.200 0.02 Matrix Spike -EPA 200. 7 QC Sample ID: BWE0432-MSl Batch: BWE0432 QC Source Sample: XXXXXXX-XX Date Prepared: 05/09/2022 Date Analyzed: 05/10/2022 Calcium, Dissolved 76.2 70-130 53.9 46.1 10.2 0.2 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Iron, Dissolved 87.4 70 -130 0.484 0.309 0.200 0.02 Magnesium, Dissolved 87.8 70 -130 17.9 9.0 10.2 0.2 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. Sodium, Dissolved 62.3 70 -130 116 110 10.0 0.5 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Tin, Dissolved CtF WO#: 22D2139 www.ChemtechFord.com 75.7 70 -130 0.15 0.002 0.200 0.02 DF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 Analyte QC Sample ID: BWE0445-MS1 Date Prepared: 05/10/2022 Calcium, Dissolved QC Report for Work Order (WO) -2202139 % Rec RPD Limits RPD Max Result Source Cone Matrix Spike -EPA 200.7 (cont.) Batch: BWE0445 QC Source Sample: 2202139-01 Date Analyzed: 05/10/2022 279 70 -130 357 328 SpkValue MRL 10.2 1.0 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. DF 5.00 Iron.Dissolved 418 70-130 0.958 0.122 0.200 0.10 5.00 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. Magnesium, Dissolved 388 70 -130 1050 1010 10.2 1.0 5.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSO due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Potassium, Dissolved 431 70 -130 59.2 16.1 10.0 2.5 5.00 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. Sodium, Dissolved 403 70 -130 275 234 10.0 2.5 5.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSO due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Tin, Dissolved 404 70 -130 0.86 0.05 0.200 0.10 5.00 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSO was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BWE0432-MS01 Date Prepared: 05/09/2022 Calcium, Dissolved Matrix Spike Dup -EPA 200.7 Batch: BWE0432 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/10/2022 51.2 4.84 70-130 20 51.3 46.1 10.2 0.2 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSO recoveries within the acceptance limits. Iron, Dissolved 79.8 3.17 70 -130 20 0.469 0.309 0.200 0.02 1.00 1.00 Magnesium, Dissolved 80.1 4.49 70 -130 20 17 .1 9.0 10.2 0.2 1.00 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. Sodium, Dissolved 11.4 4.46 70 -130 20 111 110 10.0 0.5 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSO due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSO recoveries within the acceptance limits. Tin, Dissolved QC Sample ID: BWE0445-MSD1 Date Prepared: 05/l 0/2 022 Calcium, Dissolved 76.9 1.55 70-130 20 0.16 Batch: BWE0445 QC Source Sample: 2202139-01 Date Analyzed: 05/l 0/2022 289 0.285 70 -130 20 358 0.002 0.200 0.02 328 10.2 1.0 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSO due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSO recoveries within the acceptance limits. 1.00 1.00 5.00 Iron, Dissolved 441 4.79 70-130 20 1.00 0.122 0.200 0.10 5.00 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSO was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. Magnesium, Dissolved CtF WO#: 22D2139 www.ChemtechFord.com 519 1.26 70 -130 20 1060 1010 10.2 1.0 5.00 Analyte QC Sample ID: BWE0445-MSD1 Date Prepared: 05/10/2022 QC Report for Work Order (WO) -22D2139 %Rec RPO Limits RPDMax Result Source Cone Spk Value MRL Matrix Spike Dup -EPA 200.7 (cont.) Batch: BWE0445 QC Source Sample: 22D2139-0l Date Analyzed: 05/11/2022 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. DF Potassium, Dissolved 428 0.348 70 -130 20 59.0 16.1 10.0 2.5 5.00 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. Sodium, Dissolved 416 0.460 70 -130 20 276 234 10.0 2.5 5.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Tin, Dissolved 401 0.761 70-130 20 0.85 0.05 0.200 0.10 5.00 OM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. CtF WO#: 22D2139 www.ChemtechFord.com QC Report for Work Order (WO) -22D2139 Analyte %Rec RPD Limits RPO Max Result Source Cone SpkValue MRL DF Blank -EPA 200.8 QC Sample ID: BWE0240-BLK1 Batch: BWE0240 Date Prepared: 05/04/2022 Date Analyzed: 05/05/2022 Arsenic, Dissolved ND 0.0050 1.00 Beryllium, Dissolved ND 0.0005 1.00 Cadmium, Dissolved ND 0.0005 1.00 Chromium, Dissolved ND 0.0250 1.00 Cobalt, Dissolved ND 0.010 1.00 Copper, Dissolved ND 0.0100 1.00 Lead, Dissolved ND 0.0010 1.00 Manganese, Dissolved ND 0.0100 1.00 Molybdenum, Dissolved ND 0.0100 1.00 Nickel, Dissolved ND 0.0200 1.00 Selenium, Dissolved ND 0.0050 1.00 Silver, Dissolved ND 0.010 1.00 Thallium, Dissolved ND 0.0002 1.00 Uranium, Dissolved ND 0.0003 1.00 Vanadium, Dissolved ND 0.0150 1.00 Zinc, Dissolved ND 0.01 1.00 QC Sample ID: BWE0442-BLK1 Batch: BWE0442 Date Prepared: 05/10/2022 Date Analyzed: 05/10/2022 Arsenic, Dissolved ND 0.0050 1.00 Beryllium, Dissolved ND 0.0005 1.00 Cadmium, Dissolved ND 0.0005 1.00 Chromium, Dissolved ND 0.0250 1.00 Cobalt, Dissolved ND 0.010 1.00 Copper, Dissolved ND 0.0100 1.00 Lead, Dissolved ND 0.0010 1.00 Manganese, Dissolved ND 0.0100 1.00 Molybdenum, Dissolved ND 0.0100 1.00 Nickel, Dissolved ND 0.0200 1.00 Selenium, Dissolved ND 0.0050 1.00 Silver, Dissolved ND 0.010 1.00 Thallium, Dissolved ND 0.0002 1.00 Uranium, Dissolved ND 0.0003 1.00 Vanadium, Dissolved ND 0.0150 1.00 Zinc, Dissolved ND 0.01 1.00 LCS -EPA 200.8 QC Sample ID: BWE0240-BS1 Batch: B WE0240 Date Prepared: 05/04/2022 Date Analyzed: 05/05/2022 Arsenic, Dissolved 99.7 85 -115 0.040 0.0400 0.0005 1.00 Beryllium, Dissolved 103 85 -115 0.041 0.0400 0.0005 1.00 Cadmium, Dissolved 100 85 -115 0.040 0.0400 0.0002 1.00 Chromium, Dissolved 97.7 85 -115 0.039 0.0400 0.0005 1.00 Cobalt, Dissolved 98.0 85 -115 0.039 0.0400 0.0005 1.00 Copper, Dissolved 101 85 -115 0.041 0.0400 0.0010 1.00 Lead, Dissolved 99.9 85 -115 0.040 0.0400 0.0005 1.00 Manganese, Dissolved 98.3 85 -115 0.039 0.0400 0.0005 1.00 Molybdenum, Dissolved 104 85 -115 0.042 0.0400 0.0005 1.00 Nickel, Dissolved 101 85 -115 0.0403 0.0400 0.0005 1.00 Selenium, Dissolved 102 85-115 0.041 0.0400 0.0005 1.00 Silver, Dissolved 99.0 85 -115 0.040 0.0400 0.0005 1.00 Thallium, Dissolved 101 85 -115 0.040 0.0400 0.0002 1.00 CtF WO#: 2202139 www.ChemtechFord.com QC Report for Work Order (WO) -22D2139 Analyte % Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF LCS -EPA 200.8 (cont.) QC Sample ID: BWE0240-BS1 Batch: BWE0240 Date Prepared: 05/04/2022 Date Analyzed: 05/05/2022 Uranium, Dissolved 99.4 85 -115 0.040 0.0400 0.0003 1.00 Vanadium, Dissolved 97.5 85 -115 0.039 0.0400 0.0005 1.00 Zinc, Dissolved 104 85 -115 0.04 0.0400 0.01 1.00 QC Sample ID: BWE0442-BS1 Batch: BWE0442 Date Prepared: 05/10/2022 Date Analyzed: 05/10/2022 Arsenic, Dissolved 99.1 85-115 0.040 0.0400 0.0005 1.00 Beryllium, Dissolved 103 85 -115 0.041 0.0400 0.0005 1.00 Cadmium, Dissolved 98.9 85 -115 0.040 0.0400 0.0002 1.00 Chromium, Dissolved 98.9 85 -115 0.040 0.0400 0.0005 1.00 Cobalt, Dissolved 98.4 85 -115 0.039 0.0400 0.0005 1.00 Copper, Dissolved 95.6 85 -115 0.038 0.0400 0.0010 1.00 Lead, Dissolved 106 85 -115 0.042 0.0400 0.0005 1.00 Manganese, Dissolved 96.6 85-115 0.039 0.0400 0.0005 1.00 Molybdenum, Dissolved 99.4 85-115 0.040 0.0400 0.0005 1.00 Nickel, Dissolved 91 .9 85 -115 0.0368 0.0400 0.0005 1.00 Selenium, Dissolved 100 85 -115 0.040 0.0400 0.0005 1.00 Silver, Dissolved 96.9 85 -115 0.039 0.0400 0.0005 1.00 Thallium, Dissolved 108 85-115 0.043 0.0400 0.0002 1.00 Uranium, Dissolved 106 85 -115 0.042 0.0400 0.0003 1.00 Vanadium, Dissolved 100 85 -115 0.040 0.0400 0.0005 1.00 Zinc, Dissolved 98.6 85 -115 0.04 0.0400 0.01 1.00 Matrix Spike -EPA 200.8 QC Sample ID: BWE0240-MS1 Batch: BWE0240 QC Source Sample: XXXXXXX-XX Date Prepared: 05/04/2022 Date Analyzed: 05/05/2022 Arsenic, Dissolved 104 70 -130 0.046 0.004 0.0400 0.0005 1.00 Beryllium, Dissolved 106 70 -130 0.043 0.0006 0.0400 0.0005 1.00 Cadmium, Dissolved 101 70 -130 0.040 ND 0.0400 0.0002 1.00 Chromium, Dissolved 101 70 -130 0.043 0.002 0.0400 0.0005 1.00 Cobalt, Dissolved 97.0 70 -130 0.039 0.00008 0.0400 0.0005 1.00 Copper, Dissolved 99.2 70 -130 0.074 0.035 0.0400 0.0010 1.00 Lead, Dissolved 102 70 -130 0.041 0.0004 0.0400 0.0005 1.00 Manganese, Dissolved 94.2 70 -130 0.175 0.137 0.0400 0.0005 1.00 Molybdenum, Dissolved 108 70 -130 0.045 0.002 0.0400 0.0005 1.00 Nickel, Dissolved 98.2 75 -125 0.0407 0.0015 0.0400 0.0005 1.00 Selenium, Dissolved 92.5 70 -130 0.040 0.003 0.0400 0.0005 1.00 Silver, Dissolved -0.667 70-130 0.006 0.006 0.0400 0.0005 1.00 QM-05 -The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The analytical batch was accepted based on the acceptable data provided by the Laboratory Control Sample(s) [LCS] and/or LCS Duplicates. Thallium, Dissolved 103 70 -130 0.041 ND 0.0400 0.0002 1.00 Uranium, Dissolved 102 70 -130 0.042 0.0007 0.0400 0.0003 1.00 Vanadium, Dissolved 97.2 70 -130 0.040 0.0007 0.0400 0.0005 1.00 Zinc, Dissolved 102 70 -130 0.05 0.01 0.0400 0.01 1.00 QC Sample ID: BWE0240-MS2 Batch: BWE0240 QC Source Sample: XXXXXXX-XX Date Prepared: 05/04/2022 Date Analyzed: 05/05/2022 Arsenic, Dissolved 101 70-130 0.054 0.014 0.0400 0.0005 1.00 Beryllium, Dissolved 100 70 -130 0.040 ND 0.0400 0.0005 1.00 Cadmium, Dissolved 101 70 -130 0.040 0.00004 0.0400 0.0002 1.00 Chromium, Dissolved 93.7 70 -130 0.045 0.007 0.0400 0.0005 1.00 Cobalt, Dissolved 94.0 70 -130 0.038 0.0003 0.0400 0.0005 1.00 CtF WO#: 22D2139 www.ChemtechFord.com QC Report for Work Order (WO) -2202139 Analyte %Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Matrix Spike -EPA 200.8 (cont.) QC Sample ID: BWE0240-MS2 Batch: BWE0240 QC Source Sample: XXXXXXX-XX Date Prepared: 05/04/2022. Date Analyzed: 05/05/2022 Copper, Dissolved 94.5 70 -130 0.043 0.005 0.0400 0.0010 1.00 Lead, Dissolved 101 70 -130 0.041 0.0005 0.0400 0.0005 1.00 Manganese, Dissolved 92.9 70 -130 0.063 0.026 0.0400 0.0005 1.00 Molybdenum, Dissolved 107 70 -130 0.069 0.027 0.0400 0.0005 1.00 Nickel, Dissolved 94.2 75 -125 0.0401 0.0025 0.0400 0.0005 1.00 Selenium, Dissolved 98.0 70 -130 0.043 0.004 0.0400 0.0005 1.00 Silver, Dissolved 99.0 70 -130 0.040 ND 0.0400 0.0005 1.00 Thallium, Dissolved 102 70 -130 0.041 0.00007 0.0400 0.0002 1.00 Uranium, Dissolved 100 70 -130 0.050 0.010 0.0400 0.0003 1.00 Vanadium, Dissolved 94.5 70 -130 0.042 0.005 0.0400 0.0005 1.00 Zinc, Dissolved 92.9 70 -130 0.05 0.02 0.0400 0.01 1.00 QC Sample ID: BWE0442-MSI Batch: BWE0442 QC Source Sample: XXXXXXX-XX Date Prepared: 05/l 0/2022 Date Analyzed: 05/10/2022 Arsenic, Dissolved 101 70 -130 0.041 0.0004 0.0400 0.0005 1.00 Beryllium, Dissolved 96.2 70 -130 0.038 ND 0.0400 0.0005 1.00 Cadmium, Dissolved 97.9 70 -130 0.039 ND 0.0400 0.0002 1.00 Chromium, Dissolved 97.6 70 -130 0.040 0.001 0.0400 0.0005 1.00 Cobalt, Dissolved 96.6 70 -130 0.039 0.0001 0.0400 0.0005 1.00 Copper, Dissolved 92.6 70 -130 0.040 0.003 0.0400 0.0010 1.00 Lead, Dissolved 104 70 -130 0.041 ND 0.0400 0.0005 1.00 Manganese, Dissolved 97.7 70 -130 0.039 0.0001 0.0400 0.0005 1.00 Molybdenum, Dissolved 102 70 -130 0.041 0.0002 0.0400 0.0005 1.00 Nickel, Dissolved 90.5 75 -125 0.0368 0.0006 0.0400 0.0005 1.00 Selenium, Dissolved 106 70 -130 0.042 0.0002 0.0400 0.0005 1.00 Silver, Dissolved 95.0 70-130 0.038 ND 0.0400 0.0005 1.00 Thallium, Dissolved 107 70 -130 0.043 ND 0.0400 0.0002 1.00 Uranium, Dissolved 105 70 -130 0.043 0.0006 0.0400 0.0003 1.00 Vanadium, Dissolved 98.4 70 -130 0.040 0.0007 0.0400 0.0005 1.00 Zinc, Dissolved 97.7 70 -130 0.04 ND 0.0400 0.01 1.00 QC Sample ID: BWE0442-MS2 Batch: BWE0442 QC Source Sample: 22D2139-0l Date Prepared: 05/l 0/2022 Date Analyzed: 05/10/2022 Arsenic, Dissolved 110 70 -130 0.045 0.0007 0.0400 0.0005 1.00 Beryllium, Dissolved 96.2 70 -130 0.050 0.012 0.0400 0.0005 1.00 Cadmium, Dissolved 75.7 70 -130 0.185 0.155 0.0400 0.0002 1.00 Chromium, Dissolved 87.4 70 -130 0.037 0.002 0.0400 0.0005 1.00 Cobalt, Dissolved 40.6 70 -130 0.452 0.436 0.0400 0.0005 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Copper, Dissolved 74.6 70 -130 0.123 0.094 0.0400 0.0010 1.00 Lead, Dissolved 90.1 70 -130 0.039 0.003 0.0400 0.0005 1.00 Manganese, Dissolved -3620 70 -130 49.5 50.9 0.0400 0.0250 50.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Molybdenum, Dissolved 31.6 70 -130 0.450 0.437 0.0400 0.0005 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Nickel, Dissolved 53.7 75 -125 0.274 0.253 0.0400 0.0005 1.00 CtF WO#: 22D2139 www.ChemtechFord.com Analyte QC Sample ID: BWE0442-MS2 Date Prepared: 05/10/2022 QC Report for Work Order (WO) -22D2139 %Rec RPD limits RPD Max Result Source Cone Spk Value MRL Matrix Spike -EPA 200.8 (cont.) Batch: BWE0442 QC Source Sample: 22D2139-0 I Date Analyzed: 05/10/2022 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Selenium, Dissolved 127 70 -130 0.090 0.039 0.0400 0.0005 Silver, Dissolved 87.6 70 -130 0.035 ND 0.0400 0.0005 Thallium, Dissolved 93.8 70 -130 0.040 0.002 0.0400 0.0002 Uranium, Dissolved 89.5 70 -130 0.056 0.021 0.0400 0.0003 Vanadium, Dissolved 95.4 70 -130 0.039 0.0008 0.0400 0.0005 DF 1.00 1.00 1.00 1.00 1.00 Zinc, Dissolved -42.8 70 -130 1.06 1.08 0.0400 0.01 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. CtF WO#: 22D2139 www.ChemtechFord.com Analyte QC Sample ID: BWE0045-BLKI Date Prepared: 05/02/2022 Mercury, Dissolved QC Sample ID: BWE0045-BSI Date Prepared: 05/02/2022 Mercury, Dissolved QC Sample ID: BWE0045-MSI Date Prepared: 05/02/2022 Mercury, Dissolved QC Sample ID: BWE0045-MS2 Date Prepared: 05/02/2022 Mercury, Dissolved QC Sample ID: BWE0045-MSD1 Date Prepared: 05/02/2022 Mercury, Dissolved QC Sample ID: BWE0045-MSD2 Date Prepared: 05/02/2022 Mercury, Dissolved CtF WO#: 2202139 www.ChemtechFord.com QC Report for Work Order (WO) -22D2139 %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 245.1 Batch: BWE0045 Date Analyzed: 05/04/2 022 ND 0.0005 1.00 LCS -EPA 245.1 Batch: BWE0045 Date Analyzed: 05/04/2022 97.3 85 -115 0.0049 0.00500 0.0002 1.00 Matrix Spike -EPA 245.1 Batch: BWE0045 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/04/2022 101 75 -125 0.0051 ND 0.00500 0.0002 1.00 Batch: BWE0045 QC Source Sample: 22D2139-0l Date Analyzed: 05/04/2022 98.6 75 -125 0.0049 ND 0.00500 0.0002 1.00 Matrix Spike Dup -EPA 245.1 Batch: BWE0045 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/04/2022 113 10.5 75 -125 20 0.0056 ' ND 0.00500 0.0002 1.00 Batch: BWE0045 QC Source Sample: 22D2139-0l Date Analyzed: 05/04/2022 99.7 1.12 75 -125 20 0.0050 ND 0.00500 0.0002 1.00 QC Report for Work Order {WO) -2202139 Analyte %Rec RPO Limits RPO Max Result Source Cone Spk Value MRL Blank -EPA 300.0 QC Sample ID: BWEOl41-BLK1 Batch: BWE0141 Date Prepared: 05/04/2022 Date Analyzed: 05/04/2022 Fluoride ND 0.1 QC Sample ID: BWE0358-BLK1 Batch: BWE0358 Date Prepared: 05/07/2022 Date Analyzed: 05/08/2022 Chloride ND 1.0 Sulfate ND 1.0 QC Sample ID: BWE0380-BLK1 Batch: BWE0380 Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Chloride ND 1.0 QC Sample ID: BWE1099-BLKI Batch: BWEI099 Date Prepared: 05/24/2022 Date Analyzed: 05/24/2022 Sulfate ND 1.0 LCS -EPA 300.0 QC Sample ID: BWE0141-BS1 Batch: BWE0141 Date Prepared: 05/04/2022 Date Analyzed: 05/04/2022 Fluoride 108 90 -110 5.4 5.00 0.1 QC Sample ID: BWE0358-BS I Batch: BWE0358 Date Prepared: 05/07/2022 Date Analyzed: 05/08/2022 Chloride 100 90 -110 50.1 50.0 1.0 Sulfate 101 90 -110 50.5 50.0 1.0 QC Sample ID: BWE0380-BSI Batch: BWE0380 Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Chloride 100 90 -110 50.0 50.0 1.0 QC Sample ID: BWEI099-BSI Batch: B WE 1099 Date Prepared: 05/24/2022 Date Analyzed: 05/24/2022 Sulfate 96.8 90 -110 48.4 50.0 1.0 Matrix Spike -EPA 300.0 QC Sample ID: BWE0141 -MS1 Batch: BWE0141 QC Source Sample: 22D2139-01 Date Prepared: 05/04/2022 Date Analyzed: 05/04/2022 Fluoride 52.3 80 -120 63.0 10.8 100 11 .0 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BWE0141-MS2 Batch: BWE0141 QC Source Sample: XXXXXXX-XX Date Prepared: 05/04/2022 Date Analyzed: 05/04/2022 Fluoride 102 80 -120 22.1 1.8 20.0 2.2 QC Sample ID: BWE0358-MS1 Batch: BWE0358 QC Source Sample: 22D2139-0l Date Prepared: 05/07/2022 Date Analyzed: 05/08/2022 Chloride 114 80 -120 1190 51 .8 1000 110 Sulfate 150 80 -120 7540 6040 1000 110 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWE0358-MS2 Date Prepared: 05/07/2022 Chloride Sulfate CtF WO#: 2202139 www.ChemtechFord.com Batch: BWE0358 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/08/2022 91 .2 80 -120 736 553 104 80 -120 328 120 200 200 22.0 22.0 OF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 Analyte QC Sample ID: BWE0380-MSI Date Prepared: 05/09/2022 Chloride QC Sample ID: BWE0380-MS2 Date Prepared: 05/09/2022 Chloride QC Sample ID: BWEI099-MSI Date Prepared: 05/24/2022 Sulfate QC Sample ID: BWEOI41-MSDI QC Report for Work Order (WO) -2202139 %Rec RPD Limits RPD Max Result Source Cone Matrix Spike -EPA 300.0 (cont.) Batch: BWE0380 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/09/2022 108 80 -120 6610 5530 Batch: BWE0380 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/09/2022 104 80-120 5600 4560 Batch: BWEI099 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/24/2022 96.4 80 -120 8140 3320 Matrix Spike Dup -EPA 300.0 Batch: BWEOI41 QC Source Sample: 22D2139-0l Date Prepared: 05/04/2022 Date Analyzed: 05/04/2022 SpkValue 1000 1000 5000 Fluoride 64.2 17.4 80-120 20 75.0 10.8 100 MRL 110 110 550 11.0 QM-RPD -The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPD. QC Sample ID: BWEOI41-MSD2 Date Prepared: 05/04/2022 Fluoride QC Sample ID: BWE0358-MSD1 Date Prepared: 05/07/2022 Chloride Sulfate Batch: BWEOI41 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/04/2022 101 0.199 80-120 20 22.0 1.8 Batch: BWE0358 QC Source Sample: 22D2139-0l Date Analyzed: 05/08/2022 95.2 17.3 80-120 20 1000 51.8 144 0.783 80 -120 20 7480 6040 20.0 1000 1000 2.2 110 110 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWE0358-MSD2 Date Prepared: 05/07/2022 Chloride Sulfate QC Sample ID: BWE0380-MSD1 Date Prepared: 05/09/2022 Chloride QC Sample ID: BWE0380-MSD2 Date Prepared: 05/09/2022 Chloride QC Sample ID: BWE1099-MSD1 Date Prepared: 05/24/2022 Sulfate CtF WO#: 22D2139 www.ChemtechFord.com Batch: BWE0358 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/08/2022 82.1 2.51 80 -120 20 718 553 200 22.0 96.4 4.70 80 -120 20 313 120 200 22.0 Batch: BWE0380 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/09/2022 105 0.417 80 -120 20 6580 5530 1000 110 Batch: BWE0380 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/09/2022 102 0.432 80 -120 20 5580 4560 1000 110 Batch: BWEI099 QC Source Sample: :XXXXXXX-XX Date Analyzed: 05/24/2022 97.1 0.436 80 -120 20 8170 3320 5000 550 DF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 Analyte QC Sample ID: BWE0548-BLK1 Date Prepared: 05/11/2022 Ammonia as N QC Sample ID: BWE0548-BS1 Date Prepared: 05/11/2022 Ammonia as N QC Sample ID: BWE0548-MS1 Date Prepared: 05/11/2022 Ammonia as N QC Sample ID: BWE0548-MSD1 Date Prepared: 05/11/2022 Ammonia as N CtF WO#: 22D2139 www.ChemtechFord.com QC Report for Work Order (WO) -2202139 %Rec RPO Limits RPO Max Result Source Cone Blank -EPA 350.1 Batch: BWE0548 Date Analyzed: 05/12/2022 ND LCS -EPA 350.1 Batch: BWE0548 Date Analyzed: 05/12/2022 95.1 90 -110 0.95 Matrix Spike -EPA 350.1 Batch: BWE0548 QC Source Sample: 22D2l39-01 Date Analyzed: 05/12/2022 103 80 -120 1.88 0.85 Matrix Spike Dup -EPA 350.1 Batch: BWE0548 QC Source Sample: 22D2l39-0I Date Analyzed: 05/12/2022 104 0.429 80 -120 20 1.89 0.85 SpkValue MRL OF 0.05 1.00 1.00 0.05 1.00 1.00 0.2 5.00 1.00 0.2 5.00 Analyte QC Sample ID: BWD1312-BLK1 Date Prepared: 04/29/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWD1312-BS1 Date Prepared: 04/29/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWD1312-MS1 Date Prepared: 04/29/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWD1312-MS2 Date Prepared: 04/29/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWD1312-MSD1 Date Prepared: 04/29/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWD1312-MSD2 Date Prepared: 04/29/2022 Nitrate + Nitrite, Total, as N CtF WO#: 22D2139 www.ChemtechFord.com QC Report for Work Order (WO) -22D2139 %Rec RPD Limits RPD Max Result Source Cone Blank -EPA 353.2 Batch: BWD1312 Date Analyzed: 04/29/2022 ND LCS -EPA 353.2 Batch: BWD1312 Date Analyzed: 04/29/2022 97.5 80 -120 2.0 Matrix Spike -EPA 353.2 Batch: BWD1312 QC Source Sample: 22D2139-0l Date Analyzed: 04/30/2022 90.7 80 -120 2.7 1.8 Batch: BWD1312 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/30/2022 86.5 80 -120 0.9 ND Matrix Spike Dup -EPA 353.2 Batch: BWD1312 QC Source Sample: 22D2139-0l Date Analyzed: 04/30/2022 95.6 1.78 80 -120 20 2.8 1.8 Batch: BWD1312 QC Source Sample: XXXXXXX-XX Date Analyzed: 04/30/2022 85.2 1.51 80 -120 20 0.9 ND SpkValue MRL DF 0.1 1.00 2.00 0.1 1.00 1.00 0.1 1.00 1.00 0.1 1.00 1.00 0.1 1.00 1.00 0.1 1.00 QC Report for Work Order (WO) -2202139 Analyte % Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Blank -EPA 82600 /5030A QC Sample ID: BWEOI59-BLK1 Batch: BWEOI59 Date Prepared: 05/03/2022 Date Analyzed: 05/03/2022 Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 LCS -EPA 82600 /5030A QC Sample ID: BWE0159-BS1 Batch: BWEOI59- Date Prepared: 05/03/2022 Date Analyzed: 05/03/2022 Acetone 105 80 -120 105 100 10.0 1.00 Benzene 94.3 80 -120 9.43 10.0 1.0 1.00 Carbon Tetrachloride 96.6 80 -120 9.66 10.0 1.0 1.00 Chloroform 91 .9 80 -120 9.19 10.0 1.0 1.00 Chloromethane 93.0 80 -120 9.30 10.0 1.0 1.00 Methyl Ethyl Ketone 120 80 -120 120 100 10.0 1.00 Methylene Chloride 109 80 -120 10.9 10.0 1.0 1.00 Naphthalene 104 80 -120 10.4 10.0 1.0 1.00 Tetrahydrofuran 80-120 ND 10.0 1.0 1.00 Toluene 97.4 80 -120 9.74 10.0 1.0 1.00 Xylenes, total 98.1 80 -120 29.4 30.0 1.0 1.00 Matrix Spike -EPA 82600 /5030A QC Sample ID: BWE0159-MS1 Batch: B WEO 159 QC Source Sample: 22D2139-0l Date Prepared: 05/03/2022 Date Analyzed: 05/03/2022 Acetone 103 70 -130 516 ND 500 50.0 1.00 Benzene 93.6 70 -130 46.8 ND 50.0 5.0 1.00 Carbon Tetrachloride 91 .1 70 -130 45.6 ND 50.0 5.0 1.00 Chloroform 90.1 70-130 45.0 ND 50.0 5.0 1.00 Chloromethane 91 .9 70 -130 46.0 ND 50.0 5.0 1.00 Methyl Ethyl Ketone 124 70-130 620 ND 500 50.0 1.00 Methylene Chloride 101 70 -130 50.6 ND 50.0 5.0 1.00 Naphthalene 104 70 -130 51.9 ND 50.0 5.0 1.00 Tetrahydrofuran 70 -130 ND ND 50.0 5.0 1.00 Toluene 93.7 70-130 46.8 ND 50.0 5.0 1.00 Xylenes, total 95.7 70 -130 144 ND 150 5.0 1.00 Matrix Spike Oup -EPA 82600 /5030A QC Sample ID: BWE0159-MSD1 Batch: BWE0159 QC Source Sample: 22D2I39-0l Date Prepared: 05/03/2022 Date Analyzed: 05/03/2022 Acetone 105 1.35 70 -130 20 523 ND 500 50.0 1.00 Benzene 94.3 0.745 70 -130 20 47.2 ND 50.0 5.0 1.00 Carbon Tetrachloride 96.6 5.86 70 -130 20 48.3 ND 50.0 5.0 1.00 Chloroform 93.2 3.38 70-130 20 46.6 ND 50.0 5.0 1.00 Chloromethane 98.7 7.14 70 -130 20 49.4 ND 50.0 5.0 1.00 Methyl Ethyl Ketone 113 8.87 70 -130 20 567 ND 500 50.0 1.00 Methylene Chloride 106 4.35 70 -130 20 52.8 ND 50.0 5.0 1.00 CtF WO#: 2202139 www.ChemtechFord.com Analyte QC Sample ID: BWE0159-MSD1 Date Prepared: 05/03/2022 Naphthalene Tetrahydrofuran Toluene Xylenes, total CtF WO#: 22D2139 www.ChemtechFord.com QC Report for Work Order (WO) -2202139 %Rec RPD Limits RPDMax Result Source Cone Matrix Spike Oup -EPA 82600 /5030A (cont.) Batch: BWE0159 QC Source Sample: 22D2139-0l Date Analyzed: 05/03/2022 103 0.483 70-130 20 51.6 ND 70 -130 20 ND ND 96.6 3.05 70-130 20 48.3 ND 97.6 2.00 70 -130 20 146 ND Spk Value MRL DF 50.0 5.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 150 5.0 1.00 Analyte QC Sample ID: BWE0090-BLKI Date Prepared: 05/03/2022 Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) QC Sample ID: BWE0092-BLKI Date Prepared: 05/03/2022 Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) QC Sample ID: BWE0090-DUP1 Date Prepared: 05/03/2022 Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Alkalinity -Total (as CaC03) QC Sample ID: BWE0092-DUP1 Date Prepared: 05/03/2022 Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Alkalinity -Total (as CaC03) QC Sample ID: BWE0090-BS1 Date Prepared: 05/03/2022 Alkalinity -Total (as CaC03) QC Sample ID: BWE0092-BSI Date Prepared: 05/03/2022 Alkalinity -Total (as CaC03) CtF WO#: 22D2139 www.ChemtechFord.com QC Report for Work Order (WO) -2202139 % Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Blank -SM 2320 B Batch: BWE0090 Date Analyzed: 05/03/2022 ND 1.0 1.00 ND 1.0 1.00 Batch: BWE0092 Date Analyzed: 05/03/2022 ND 1.0 1.00 ND 1.0 1.00 Duplicate -SM 2320 B Batch: B WE0090 QC Source Sample: 22D2139-0l Date Analyzed: 05/03/2022 20 ND ND 1.0 1.00 20 ND ND 1.0 1.00 20 ND ND 1.0 1.00 Batch: BWE0092 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/03/2022 0.00 20 58.8 58.8 1.0 1.00 20 ND ND 1.0 1.00 0.00 20 58.8 58.8 1.0 1.00 LCS -SM 2320 B Batch: BWE0090 Date Analyzed: 05/03/2022 102 90 -110 240 236 1.0 1.00 Batch: BWE0092 Date Analyzed: 05/03/2022 103 90 -110 243 236 1.0 1.00 Analyte QC Sample ID: BWE0025-BLK1 Date Prepared: 05/02/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0025-BS1 Date Prepared: 05/02/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0025-DUP1 Date Prepared: 05/02/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0025-DUP2 Date Prepared: 05/02/2022 Total Dissolved Solids (TDS) QC Report for Work Order (WO) -22D2139 %Rec RPO Limits RPD Max Result Source Cone Batch: BWE0025 Date Analyzed: 05/02/2022 ND Batch: BWE0025 Date Analyzed: 05/02/2022 98 90 -110 392 Batch: BWE0025 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/02/2022 7 10 700 752 Batch: BWE0025 QC Source Sample: 22D2139-0I Date Analyzed: 05/02/2022 29 10 8980 12000 Spk Value MRL 10 400 20 20 100 QM-02 -The RPO and/or percent recovery for this QC spike sample cannot be accurately calculated due to the high concentration of analyte inherent in the sample. QC Sample ID: BWE0026-BLK1 Batch: BWE0026 Date Prepared: 05/02/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0026-BS1 Date Prepared: 05/02/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0026-DUP1 Date Prepared: 05/02/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0026-DUP2 Date Prepared: 05/02/2022 Total Dissolved Solids (TDS) CtF WO#: 22D2139 www.ChemtechFord.com Date Analyzed: 05/02/2022 ND Batch: BWE0026 Date Analyzed: 05/02/2022 99 90-110 396 Batch: BWE0026 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/02/2022 9 10 1~ 1~ Batch: BWE0026 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/02/2022 3 10 43100 44400 10 400 20 20 500 DF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 9632 South 500 West CHEMTECH·FORD LA60RATORIES Amended 6/3/2022 Work Order: 22E 1503 Project: 2nd Quarter Ground Water 2022 Energy Fuels Resources, Inc. Attn: Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Client Service Contact: 801.262.7299 The analyses presented on this report were performed in accordance with the National Environmental Laboratory Accreditation Program (NELAP) unless noted in the comments, flags, or case narrative. If the report is to be used for regulatory compliance, it should be presented in its entirety, and not be altered. Approved By: Melissa Connolly, Project Manager Sandy, Utah 84070 801 .262.7299 Main 666.792.0093 Fax SeNing the lntermountain West since 1953 www.ChemtechFord.com CHEMTECH-FORD LABORATORIES Energy Fuels Resources, Inc. Project: 2nd Quarter Ground Water 2022 Project Manager: Tanner Holliday Laboratory ID 22E1503-01 22E1503-02 22E1503-03 22E1503-04 22E1503-05 Sample Name MW-20_05172022 MW-37 _05172022 MW-27_05162022 MW-32_05162022 Trip Blank Work Order Report Narrative Amended. Report Comments The sample time on 22E1503-05 has been corrected. Surrogate recoveries have been added to the report. TDS Ratio Comments The TDS Ratio reported on 22E1503-03 and 22E1503-04 were calculated from the TDS analyzed for 22E1503, and the TDS, Calculated from 2201197. Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions There are no corrective actions associated with this work order. Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 22E1503 I CHEMTECH·FORD lAS0R>\1'0RIES Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Amended Certificate of Analysis Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations ND = Not detected at the corresponding Minimum Reporting Limit (MRL). PO#: Receipt: 5/18/22 12:20@ 0.8 °C Date Reported: 6/3/2022 Project Name: 2nd Quarter Ground Water 2022 1 mg/L = one milligram per liter or I mg/kg = one milligram per kilogram = 1 part per million. 1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = I part per billion. I ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion Flag Descriptions J-LOW = Estimated low due to low recovery of LCS or CCV Project Name: 2nd Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 22E1503 Page 10 of24 .:1 American West Analytical Laboratories 463 W. 3600 S. Seit Lake City, UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 L~ Fax# (801) 263-8687 Email awal@awal-labs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: Email: tholllda~41aeqyfaelll.com; lnremel@elleqyfaela.com Project Name: 2nd Quarter Ground Water 2022 Project#: PO#: Sampler Name: Tanner Holliday Date Samele ID: Samcled IIW-20 0!5172022 !5/17/2022 ! IIW-37 0!5172022 C2 (\3 !5/17/2022 -_j41 ()5 7 8 9 r I ' I) I :1 IIW-27 _0!5162022 IIW-32_05162022 TRIPBLA11X I~.,.,.:.:)---·--ilJJ 'L " e ·~ •• """'Name: TANNER HOUIOAY -....j R~by. ""'nalln IDri"'Name: ~elinqulshed by: "'"nallre Print Name: Rellnqulshedby: 1 ..... _ F'nnlName: !5/16/2022 !5/16/2022 5/17/2022 IU""' S/17 rrrnw. 111V Dale: rime: ~ate: ITime: Dace: 111me: CHAIN OF CUSTODY 2 ~ c:-/5 03 All analysis will be conducted using NElAP aca,,dlted mettods..., an data will be reported using AWAL's standard ana1y1e lls., and AWAL lab Semple Set# reporting limits (POI.) LneSS ~ requested olhetWise on INs Chain of CuslDdy and/or attached docunentallon Page 1 ar 1 I QC Level: I Tum Around Time: Unless olher am,ngemenl!I have been m-. l°ooo.,,. I signed reports wtl be emaled by 5:00 pm on 3 Standard the day !hey .... due. K Include EDD: Laboratory Use Only 0 LOCUS UPLOAD :E as u EXCEL ~Wen,: oii bO K Field Filtered For: GM-~ ~ :r: ::. Dmomd lletala .... i:: II) :. :i 2 ~~ "I" C'I .ti oi ~ a.. z For Compliance With: 3 n,mpera1,1re Uc J" 1'C c:i .; t!i-0 NELAP C r.. 0 RCRA o' c-. i >' 0 CWA RoceM<f 8n>l<er,'lw:lr1g c:i ;:::. 4 C c:i u :i 0 SOWA (lmprope,ty SeeledJ ~ "l ci 0 ELAP/A2LA y N .... ~ C .. ~ u d ~ 0 C rn 0 NLLAP ;:;;-C c-. -! .: 0 Non~ompliance 5 Pn,per1y PreseM!d "l C "l u {:: ~ ... II) ~ ... 0 Other: y N 0 ~ • 'O oii G' e? ~ C, G' 1 II u < • C Checl<ed at bench .. X C § C u IO y N C :s I'> C "I" u .,, .; .; ~ C'I ~ .. 0 II) II) iii • al rn ~ 6 RoceM!dWill>in 5 :::;; Ir: ~ ~ ! -; Known Hazards ., -tf -0 ,i z Ill • Holding Tlmes Time 0 D. " I'> ID 1 i < 8 & 0 E 0 ; .: ~ a y N Sampled .. Ir: u 0 > Sample Comments .. Cl) ... 800 7 w X X X X X X X X X X 830 7 w X X X X X X X X X X COCTapeWM: 11!50 1 w 1 Presenl on °'*"° P8Cl:agG X 0 N NA 1220 l w X 2 Unbroil"' on o.Aor Pe<:uge 800 3 w X (j N NA y N 3 Present on sample 6 4 UrorokenonSample G y N -Sample r..--COC Rl!CMI? y cJ Racelved by: Date: Special Instructions: ,,rne: """'Name: / < Sample containers for metals were field filtered. See the =~ /[ a, _/ ~s1;j?/;,~ 2--Analytical Scope of Work for Reporting Limits and voe analyte I .P! """' NM>e: ,fr" /t.._ µ~-;___/ Tlme:/_;z 7 / I list. Received by: I pate: --rnme: ~.Name. Received by: IOate: Slonab.re rnme: Print Name: Work Order # 2. J... c-/ S O 3 CHEMTECH FORD LABORATORIES Sample Receipt Delivery Method: D USPS ,,.PUPS r b FedEx o Chemtech Courier o Walle-in D Customer Courier IUI"!, \:IKUUNU TRACKING#: 1Z 187 Y4Y 03 9500 8818 I s:~. I:~:.:. r=· 1~01-. /l'i;(b R (I~¥ N ' r::; ~ <k) G/i ~t_ (', ?,. • 6'-/ ,q c./,' 0 £_ l ~/ e-1,~ f 1'1r·I: Receiving Temperature (" · ~ ~.C I ltl ·i i ilf l..,,...._1' ;.--... I~.-:-.-~.........,..,..-· -._.-,,-_ .. ~ ---,-:~ .. -. ----~ ---.. -1 Comments ., I CHEMTECH-FORD LABORATORIES Sample Condition (dlt!cklf~) i::r;.;.tody seals a1ottt~ll'\Qf'S Intact ~ U1' be matched to bottles o1'ec.eived on Ice D'torrect Containe<S(s) ~Sufficent Sample Volu!'TW! ~ad~ Present (VOCI D Temperature Blank 0 Received within Holding lime Plastic Containers A. Pl.lStr(. Un?{eSeNcd a, Miscellaneous Plastic C-Cyanide Qt (NaOH) E • Coliform/Ecoll/HPC f• Sulfide Qt (Zn Acetate) L-M•<CUJ'\'1611 M, Metals Pint (HN03) N, Nutrient Pint (H2S04) R, Radlo~I (HN03! S• Sludge Cups/Tubs Q-Pt,,.1lc e,,m Glass Containers O· 62S (NaZSZ03) G, Glass Unpreserved H· HAAs (NH4CI) J, 508/SlS/525 (Na2S03) K• 515.3 Herbicides O• Oil & Grease (HCI) P· Pnonols (H2S04) r TOC/TOX (H3P04) U• 531 (MCAA, Na2S203) V• 524/rHMS (Ascorbic Acid) w, 8260 voe (U HO) X· Vial Unpreserved v. 624/504 (Na2S203) z. Miscellaneous Glass QC Report for Work Order (WO) -22E1503 Analyte % Rec RPO Limits RPO Max Result Source Cone SpkValue MRL Blank -EPA 200.7 QC Sample ID: BWE1337-BLKI Batch: BWE1337 Date Prepared: 05/27/2022 Date Analyzed: 05/27/2022 Calcium, Dissolved ND 0.2 Iron, Dissolved ND 0.03 Magnesium, Dissolved ND 0.2 Potassium, Dissolved ND 0.5 Sodium, Dissolved ND 0.5 Tin, Dissolved ND 0.10 LCS -EPA 200. 7 QC Sample ID: BWE1337-BSI Batch: BWE1337 Date Prepared: 05/27/2022 Date Analyzed: 05/27/2022 Calcium, Dissolved 95.4 85 -115 9.7 10.2 0.2 Iron, Dissolved 128 85 -115 0.257 0.200 0.02 Magnesium, Dissolved 99.5 85 -115 10.1 10.2 0.2 Potassium, Dissolved 103 85 -115 10.3 10.0 0.5 Sodium, Dissolved 98.7 85 -115 9.9 10.0 0.5 Tin, Dissolved 98.0 85 -155 0.20 0.200 0.02 Matrix Spike -EPA 200. 7 QC Sample ID: BWE1337-MSI Batch: BWE1337 QC Source Sample: 22El503-0l Date Prepared: 05/27/2022 Date Analyzed: 05/27/2022 Calcium, Dissolved 113 70 -130 346 288 51.0 1.0 Iron, Dissolved 105 70 -130 1.05 ND 1.00 0.10 QM-11 -The Laboratory Control Sample recovery was outside acceptance limits. The analytical batch was accepted based on the recovery of the Method Spike. Magnesium, Dissolved 105 70 -130 84.7 31.2 51.0 1.0 Potassium, Dissolved 109 70 -130 79.1 24.3 50.0 2.5 Sodium, Dissolved 146 70 -130 1160 1080 50.0 2.5 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Tin, Dissolved QC Sample ID: BWE1337-MSDI Date Prepared: 05/27/2022 Calcium, Dissolved 98.9 70-130 1.01 0.02 Matrix Spike Dup -EPA 200. 7 Batch: BWE1337 QC Source Sample: 22El503-0l Date Analyzed: 05/27/2022 110 0.364 70 -130 20 344 288 1.00 0.10 51.0 1.0 Iron, Dissolved 107 1.37 70 -130 20 1.07 ND 1.00 0.10 QM-11 -The Laboratory Control Sample recovery was outside acceptance limits. The analytical batch was accepted based on the recovery of the Method Spike. Magnesium, Dissolved Potassium, Dissolved Sodium, Dissolved 104 109 139 0.513 0.124 0.293 70 -130 70 -130 70 -130 20 20 20 84.3 79.0 1150 31.2 24.3 1080 51.0 50.0 50.0 1.0 2.5 2.5 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Tin, Dissolved 98.6 0.24 7 70 -130 20 1.01 0.02 1.00 0.1 O CtF WO#: 22E1503 www.ChemtechFord.com OF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 QC Report for Work Order (WO) -22E1503 Analyte %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 200.8 QC Sample ID: BWEI338-BLKI Batch: BWEI338 Date Prepared: 05 /27/2022 Date Analyzed: 05/27/2022 Arsenic, Dissolved ND 0.0050 1.00 Beryllium, Dissolved ND 0.0005 1.00 Cadmium, Dissolved ND 0.0005 1.00 Chromium, Dissolved ND 0.0250 1.00 Cobalt, Dissolved ND 0.010 1.00 Copper, Dissolved ND 0.0100 1.00 Lead, Dissolved ND 0.0010 1.00 Manganese, Dissolved ND 0.0100 1.00 Molybdenum, Dissolved ND 0.0100 1.00 Nickel, Dissolved ND 0.0200 1.00 Selenium, Dissolved ND 0.0050 1.00 Silver, Dissolved ND 0.010 1.00 Thallium, Dissolved ND 0.0002 1.00 Uranium, Dissolved ND 0.0003 1.00 Vanadium, Dissolved ND 0.0150 1.00 Zinc, Dissolved ND 0.01 1.00 LCS -EPA 200.8 QC Sample ID: BWEI338-BSI Batch: BWE1338 Date Prepared: 05/27/2022 Date Analyzed: 05/27/2022 Arsenic, Dissolved 103 85 -115 0.041 0.0400 0.0005 1.00 Beryllium, Dissolved 98.9 85 -115 0.040 0.0400 0.0005 1.00 Cadmium, Dissolved 101 85 -115 0.040 0.0400 0.0002 1.00 Chromium, Dissolved 102 85 -115 0.041 0.0400 0.0005 1.00 Cobalt, Dissolved 101 85 -115 0.040 0.0400 0.0005 1.00 Copper, Dissolved 97.4 85 -115 0.039 0.0400 0.0010 1.00 Lead, Dissolved 107 85 -115 0.043 0.0400 0.0005 1.00 Manganese, Dissolved 103 85 -115 0.041 0.0400 0.0005 1.00 Molybdenum, Dissolved 102 85 -115 0.041 0.0400 0.0005 1.00 Nickel, Dissolved 96.0 85 -115 0.0384 0.0400 0.0005 1.00 Selenium, Dissolved 104 85 -115 0.042 0.0400 0.0005 1.00 Silver, Dissolved 98.9 85 -115 0.040 0.0400 0.0005 1.00 Thallium, Dissolved 113 85 -115 0.045 0.0400 0.0002 1.00 Uranium, Dissolved 109 85 -115 0.044 0.0400 0.0003 1.00 Vanadium, Dissolved 101 85 -115 0.040 0.0400 0.0005 1.00 Zinc, Dissolved 102 85 -115 0.04 0.0400 0.01 1.00 Matrix Spike -EPA 200.8 QC Sample ID: BWEI338-MSI Batch: BWE1338 QC Source Sample: 22El503-0I Date Prepared: 05/27/2022 Date Analyzed: 05/27/2022 Arsenic, Dissolved 109 70 -130 0.047 0.004 0.0400 0.0005 1.00 Beryllium, Dissolved 93.4 70 -130 0.037 ND 0.0400 0.0005 1.00 Cadmium, Dissolved 96.9 70 -130 0.039 0.00007 0.0400 0.0002 1.00 Chromium, Dissolved 92.6 70 -130 0.040 0.003 0.0400 0.0005 1.00 Cobalt, Dissolved 89.3 70 -130 0.036 0.0004 0.0400 0.0005 1.00 Copper, Dissolved 80.4 70 -130 0.034 0.002 0.0400 0.0010 1.00 Lead, Dissolved 94.6 70 -130 0.038 ND 0.0400 0.0005 1.00 Manganese, Dissolved 93.1 70 -130 0.038 0.0005 0.0400 0.0005 1.00 Molybdenum, Dissolved 110 70 -130 0.058 0.014 0.0400 0.0005 1.00 Nickel, Dissolved 81.4 75 -125 0.0349 0.0023 0.0400 0.0005 1.00 Selenium, Dissolved 120 70-130 0.051 0.003 0.0400 0.0005 1.00 Silver, Dissolved 97.1 70 -130 0.039 ND 0.0400 0.0005 1.00 CtF WO#: 22E1503 www.ChemtechFord.com Analyte QC Sample ID: BWEl338-MSI Date Prepared: 05/27/2022 Thallium, Dissolved Uranium, Dissolved Vanadium, Dissolved Zinc, Dissolved CtF WO#: 22E1503 www.ChemtechFord.com QC Report for Work Order (WO) -22E1503 %Rec RPD Limits RPD Max Result Source Cone Matrix Spike -EPA 200.8 (cont.) Batch: BWEI338 QC Source Sample: 22£1503-01 Date Analyzed: 05/27/2022 103 70 -130 0.041 ND 106 70-130 0.044 0.002 96.3 70 -130 0.047 0.009 83.8 70 -130 0.04 0.004 SpkValue MRL DF 0.0400 0.0002 1.00 0.0400 0.0003 1.00 0.0400 0.0005 1.00 0.0400 0.01 1.00 Analyte QC Sample ID: BWE0898-BLKI Date Prepared: 05/18/2022 Mercury, Dissolved QC Sample ID: BWE0898-BS1 Date Prepared: 05/18/2022 Mercury, Dissolved QC Sample ID: BWE0898-MS I Date Prepared: 05/18/2022 Mercury, Dissolved QC Sample ID: BWE0898-MSDI Date Prepared: 05/18/2022 Mercury, Dissolved CtF WO#: 22E1503 www.ChemtechFord.com QC Report for Work Order (WO) -22E1503 %Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Blank -EPA 245.1 Batch: BWE0898 Date Analyzed: 05/20/2022 ND 0.0005 1.00 LCS -EPA 245.1 Batch: BWE0898 Date Analyzed: 05/20/2022 103 85-115 0.0052 0.00500 0.0002 1.00 Matrix Spike -EPA 245.1 Batch: BWE0898 QC Source Sample: 22EI503-0l Date Analyzed: 05/20/2022 86.7 75 -125 0.0043 ND 0.00500 0.0002 1.00 Matrix Spike Dup -EPA 245.1 Batch: BWE0898 QC Source Sample: 22El503-01 Date Analyzed: 05/20/2022 92.6 6.59 75 -125 20 0.0046 ND 0.00500 0.0002 1.00 QC Report for Work Order (WO) -22E1503 Analyte %Rec RPO Limits RPO Max Result Source Cone Spk Value MRL QC Sample ID: BWE1196-BLKI Date Prepared: 05/25/2022 Chloride Fluoride QC Sample ID: BWE1452-BLKI Date Prepared: 05/31/2022 Sulfate QC Sample ID: BWE1196-BSI Date Prepared: 05/25/2022 Chloride Fluoride QC Sample ID: BWE1452-BS1 Date Prepared: 05/31/2022 Sulfate QC Sample ID: BWE1196-MSl Date Prepared: 05/25/2022 Chloride Fluoride QC Sample ID: BWE1196-MS2 Date Prepared: 05/25/2022 Chloride Blank -EPA 300.0 Batch: BWE1196 Date Analyzed: 05/25/2022 Batch: BWE1452 Date Analyzed: 05/31/2022 LCS -EPA 300.0 Batch: BWEI 196 Date Analyzed: 05/25/2022 100 90 -110 91.6 90 -110 Batch: BWE1452 Date Analyzed: 05/31/2022 96.7 90 -110 Matrix Spike -EPA 300.0 ND ND ND 50.1 4.6 48.4 Batch: BWE1196 QC Source Sample: 22El503-0l Date Analyzed: 05/25/2022 98.5 80 -120 71.8 81.8 80 -120 1.1 60.9 0.2 Batch: BWEl 196 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/25/2022 -276000 80-120 0.7 30600 50.0 5.00 50.0 11.1 1.11 11.1 1.0 0.1 1.0 1.0 0.1 1.0 1.1 0.1 1.1 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). OF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 Fluoride 19.5 80-120 0.2 ND 1.11 0.1 1.00 QM-05 -The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The analytical batch was accepted based on the acceptable data provided by the Laboratory Control Sample(s) [LCS] and/or LCS Duplicates. QC Sample ID: BWE1452-MS1 Batch: BWE1452 QC Source Sample: 22E1503-01 Date Prepared: 05/31/2022 Date Analyzed: 05/31/2022 Sulfate 106 80 -120 3880 2820 1000 110 Matrix Spike Dup -EPA 300.0 QC Sample ID: BWEI 196-MSDl Batch: BWE1196 QC Source Sample: 22El503-0l Date Prepared: 05/25/2022 Date Analyzed: 05/25/2022 Chloride 101 0.460 80 -120 20 72.2 60.9 11.1 1.1 Fluoride 85.7 3.95 80-120 20 1.1 0.2 1.11 0.1 QC Sample ID: BWEI l 96-MSD2 Batch: BWE1196 QC Source Sample: XXXXXXX-XX Date Prepared: 05/25/2022 Date Analyzed: 05/25/2022 Chloride -276000 80 -120 20 4.0 30600 11.1 1.1 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). 1.00 1.00 1.00 1.00 Fluoride 23.6 19.0 80 -120 20 0.3 ND 1.11 0.1 1.00 QM-05 -The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The analytical batch was accepted based on the acceptable data provided by the Laboratory Control Sample(s) [LCS] and/or LCS Duplicates. CtF WO#: 22E1503 www.ChemtechFord.com Analyte QC Sample ID: BWE1452-MSD1 Date Prepared: 05/31/2022 Sulfate CtF WO#: 22E1503 www.ChemtechFord.com QC Report for Work Order (WO) -22E1503 %Rec RPO Limits RPO Max Result Source Cone Matrix Spike Cup -EPA 300.0 (cont.) Batch: BWE1452 QC Source Sample: 22El503-01 Date Analyzed: 05/31/2022 105 0.0474 80-120 20 3880 2820 Spk Value MRL OF 1000 110 1.00 Analyte QC Sample ID: BWEI423-BLKI Date Prepared: 05/27/2022 Ammonia as N QC Sample ID: BWE1423-BS1 Date Prepared: 05/27/2022 Ammonia as N QC Sample ID: BWEI423-MS1 Date Prepared: 05/27/2022 Ammonia as N QC Sample ID: BWE1423-MSD1 Date Prepared: 05/27/2022 Ammonia as N CtF WO#: 22E1503 www.ChemtechFord.com QC Report for Work Order (WO) -22E1503 %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 350.1 Batch: BWEI423 Date Analyzed: 05/27/2022 ND 0.05 1.00 LCS -EPA 350.1 Batch: BWE1423 Date Analyzed: 05/27/2022 102 90 -110 1.02 1.00 0.05 1.00 Matrix Spike -EPA 350.1 Batch: BWEI423 QC Source Sample: 22EI503-0l Date Analyzed: 05/27/2022 99.1 80 -120 0.99 ND 1.00 0.05 1.00 Matrix Spike Dup -EPA 350.1 Batch: BWE1423 QC Source Sample: 22El503-0l Date Analyzed: 05/27/2022 108 8.84 80 -120 20 1.08 ND 1.00 0.05 1.00 QC Report for Work Order (WO) -22E1503 Analyte %Rec RPD Limits RPD Max Result Source Cone SpkValue Blank -EPA 353.2 QC Sample ID: BWEl 114-BLKl Batch: BWEll 14 Date Prepared: 05/24/2022 Date Analyzed: 05/24/2022 Nitrate+ Nitrite, Total, as N ND LCS -EPA 353.2 QC Sample ID: BWE1114-BS1 Batch: BWEl 114 Date Prepared: 05/24/2022 Date Analyzed: 05/24/2022 Nitrate + Nitrite, Total, as N 102 80 -120 2.0 2.00 Matrix Spike -EPA 353.2 QC Sample ID: BWEl 114-MSl Batch: BWEI 114 QC Source Sample: XXXXXXX-XX Date Prepared: 05/24/2022 Date Analyzed: 05/24/2022 Nitrate + Nitrite, Total, as N 90.8 80 -120 1.0 0.08 1.00 QC Sample ID: BWE1114-MS2 Batch: BWE1114 QC Source Sample: 22El503-0l Date Prepared: 05/24/2022 Date Analyzed: 05/24/2022 Nitrate + Nitrite, Total, as N 76.5 80-120 8.9 8.2 1.00 QM-12 -The MSD recovery was outside acceptance limits, but passed duplicate spike acceptance criteria. The batch was accepted based on the acceptability of the MS. QC Sample ID: BWEl 114-MSDI Date Prepared: 05/24/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWE1114-MSD2 Date Prepared: 05/24/2022 Nitrate+ Nitrite, Total, as N CtF WO#: 22E1503 www.ChemtechFord.com Matrix Spike Dup -EPA 353.2 Batch: BWE1114 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/24/2022 85.8 5.19 80 -120 20 0.9 0.08 Batch: BWEI114 QC Source Sample: 22£1503-01 Date Analyzed: 05/24/2022 96.9 2.26 80 -120 20 9.1 8.2 1.00 1.00 MRL DF 0.1 1.00 0.1 1.00 0.1 1.00 0.5 5.00 0.1 1.00 0.5 5.00 QC Report for Work Order (WO) -22E1503 Analyte % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL Blank -EPA 82600 /5030A QC Sample ID: BWE1260-BLK1 Batch: BWE1260 Date Prepared: 05/25/2022 Date Analyzed: 05/25/2022 Acetone ND 20.0 J-LOW -Estimated low due to low recovery of LCS or CCV Benzene ND 1.0 Carbon Tetrachloride ND 1.0 Chloroform ND 1.0 Chloromethane ND 1.0 J-LOW -Estimated low due to low recovery of LCS or CCV Methyl Ethyl Ketone ND 20.0 Methylene Chloride ND 1.0 Naphthalene ND 1.0 Tetrahydrofuran ND 1.0 Toluene ND 1.0 Xylenes, total ND 1.0 LCS -EPA 82600 /5030A QC Sample ID: BWE1260-BS1 Batch: BWE1260 Date Prepared: 05/25/2022 Date Analyzed: 05/25/2022 Acetone 68.6 70 -130 68.6 100 10.0 J-LOW -Estimated low due to low recovery of LCS or CCV Benzene 108 70 -130 10.8 10.0 1.0 Carbon Tetrachloride 97.2 70 -130 9.72 10.0 1.0 Chloroform 92.7 70 -130 9.27 10.0 1.0 Chloromethane 77.2 70 -130 7.72 10.0 1.0 J-LOW -Estimated low due to low recovery of LCS or CCV Methyl Ethyl Ketone 104 70 -130 104 100 10.0 Methylene Chloride 110 70 -130 11 .0 10.0 1.0 Naphthalene 96.5 70 -130 9.65 10.0 1.0 Tetrahydrofuran 131 70 -130 26.1 20.0 1.0 HB -Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore accepted and reported for this parameter. Toluene 105 70 -130 10.5 Xylenes, total 111 70-130 33.2 Matrix Spike -EPA 82600 /5030A QC Sample ID: BWE1260-MS1 Batch: BWE1260 QC Source Sample: 22El503-0l Date Prepared: 05 /25/2022 Date Analyzed: 05/25/2022 Acetone 69.2 70 -130 346 J-LOW -Estimated low due to low recovery of LCS or CCV Benzene 95.0 70 -130 47.5 Carbon Tetrachloride 79.4 70 -130 39.7 Chloroform 81.4 70 -130 40.7 Chloromethane 67.3 70 -130 33.6 J-LOW -Estimated low due to low recovery of LCS or CCV Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total CtF WO#: 22E1503 www.ChemtechFord.com 98.9 70-130 494 92.7 70 -130 46.4 81 .1 70 -130 40.6 124 70 -130 124 93.3 70 -130 46.6 92.8 70 -130 139 Matrix Spike Oup -EPA 82600 /5030A 10.0 1.0 30.0 1.0 ND 500 50.0 ND 50.0 5.0 ND 50.0 5.0 ND 50.0 5.0 ND 50.0 5.0 ND 500 50.0 ND 50.0 5.0 ND 50.0 5.0 ND 100 5.0 ND 50.0 5.0 ND 150 5.0 OF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 QC Report for Work Order (WO) -22E1503 Analyte %Rec RPD Limits RPDMax Result Source Cone Matrix Spike Dup -EPA 8260D /5030A (cont.) QC Sample ID: BWE1260-MSD1 Batch: BWE1260 QC Source Sample: 22El503-0l Date Prepared: 05/25/2022 Date Analyzed: 05/25/2022 Acetone 69.3 0.0867 J-LOW -Estimated low due to low recovery of LCS or CCV Benzene 92.7 2.45 Carbon Tetrachloride 78.7 0.886 Chloroform 83.9 3.02 Chloromethane 68.1 1.18 J-LOW -Estimated low due to low recovery of LCS or CCV Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total CtF WO#: 22E1503 www.ChemtechFord.com 99.4 0.535 90.8 2.07 84.4 3.99 118 5.29 92.1 1.29 93.7 0.894 70 -130 70 -130 70 -130 70 -130 70 -130 70 -130 70 -130 70 -130 70 -130 70 -130 70 -130 20 346 ND 20 46.4 ND 20 39.4 ND 20 42.0 ND 20 34.0 ND 20 497 ND 20 45.4 ND 20 42.2 ND 20 118 ND 20 46.0 ND 20 140 ND SpkValue MRL DF 500 50.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 500 50.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 100 5.0 1.00 50.0 5.0 1.00 150 5.0 1.00 Analyte QC Sample ID: BWE1131-BLK1 Date Prepared: 05/24/2022 Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) QC Sample ID: BWEl 131-DUPl Date Prepared: 05/24/2022 Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Alkalinity -Total (as CaC03) QC Sample ID: BWE1131-BSI Date Prepared: 05/24/2022 Alkalinity -Total (as CaC03) CtF WO#: 22E1503 www.ChemtechFord.com QC Report for Work Order (WO) -22E1503 % Rec RPD Limits RPDMax Result Source Cone SpkValue MRL DF Blank -SM 2320 B Batch: BWE1131 Date Analyzed: 05/24/2022 ND 1.0 1.00 ND 1.0 1.00 Duplicate -SM 2320 B Batch: BWE1131 QC Source Sample: 22El503-01 Date Analyzed: 05/24/2022 0.239 20 83.7 83.5 1.0 1.00 20 ND ND 1.0 1.00 0.239 20 83.7 83.5 1.0 1.00 LCS -SM 2320 B Batch: BWE113I Date Analyzed: 05/24/2022 91.4 90 -110 216 236 1.0 1.00 Analyte QC Sample ID: BWE0937-BLKI Date Prepared: 05/19/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0937-BS1 Date Prepared: 05/19/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0937-DUP1 Date Prepared: 05/19/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0937-DUP2 Date Prepared: 05/19/2022 Total Dissolved Solids (TDS) CtF WO#: 22E1503 www.ChemtechFord.com QC Report for Work Order (WO) -22E1503 %Rec RPD Limits RPD Max Result Source Cone SpkValue MRL DF Batch: BWE0937 Date Analyzed: 05/19/2022 ND 10 1.00 Batch: BWE0937 Date Analyzed: 05/19/2022 99 90 -110 396 400 20 1.00 Batch: BWE0937 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/19/2022 0 10 148 148 20 1.00 Batch: BWE0937 QC Source Sample: 22E1503-0l Date Analyzed: 05/19/2022 2 10 4560 4450 20 1.00 Surrogates Report for Work Order (WO) -22E1503 QCID Analyte % Rec LCL UCL Result Spk Value Blank -EPA 8260D /5030A BWE1260-BLK1 1,2-Dichloroethane-d4 84.7 64.2 126 8.47 10.0 BWE1260-BLK1 4-Bromofluorobenzene 110 71.4 122 11 .0 10.0 BWE1260-BLK1 Toluene-dB 102 63.2 129 10.2 10.0 LCS -EPA 8260D /5030A BVVE1260-BS1 1,2-Dichloroethane-d4 84.2 64.2 126 8.42 10.0 BWE1260-BS1 4-Bromofluorobenzene 113 71.4 122 11.3 10.0 BWE1260-BS1 Toluene-dB 102 63.2 129 10.2 10.0 Matrix Spike -EPA 82600 /5030A BWE1260-MS1 1,2-Dichloroethane-d4 85.6 64.2 126 42.8 50.0 BVVE1260-MS1 4-Bromofluorobenzene 106 71.4 122 53.0 50.0 BWE1260-MS1 Toluene-dB 100 63.2 129 50.0 50.0 Matrix Spike Dup -EPA 8260D /5030A BWE 1260-MS01 1,2-Dichloroethane-d4 78.9 64.2 126 39.4 50.0 BWE1260-MS01 4-Bromofluorobenzene 106 71.4 122 53.0 50.0 BWE 1260-MS01 Toluene-dB 100 63.2 129 50.0 50.0 Surrogate Recoveries (Field Samples) LabNumber Analyte Result Spklvl %Rec LCL UCL 8260 Low Level Volatiles 22E1503-01 Toluene-dB 22E1503-01 4-Bromofluorobenzene 22E1503-01 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22E1503-02 Toluene-dB 22E1503-02 22E1503-02 4-Bromofluorobenzene 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22E1503-05 Toluene-dB 22E1503-05 22E1503-05 4-Bromofluorobenzene 1,2-Dichloroethane-d4 CtF WO#: 22E1503 www.ChemtechFord.com 10.2 10.8 8.42 10.3 10.5 8.29 10.2 10.9 8.17 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 102 108 84.2 103 105 82.9 102 109 81 .7 63.2 129 71.4 122 64.2 126 63.2 129 71 .4 122 64.2 126 63.2 129 71.4 122 64.2 126 Batch OF BWE1260 1.00 BWE1260 1.00 BWE1260 1.00 BWE1260 1.00 BWE1260 1.00 BVVE1260 1.00 BWE1260 1.00 BWE1260 1.00 BWE1260 1.00 BWE1260 1.00 BWE1260 1.00 BWE1260 1.00 Qualifier lt;I 4 • I Laboratories LLC a member of The GEL Group INC PO Box30712 Charleston SC29417 2040 Sa•1age Road Charleston SC 29407 P 84~ 556.8171 F 843 766,1178 May 16, 2022 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: White Mesa Mill GW Work Order: 576962 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on April 19, 2022. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DW16I38 Enclosures Sincerely Julie Robinson Project Manager i111rn111111n n 11 111 111 , 111 11 11111 gel.com May 16, 2022 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 576962 Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on April 19, 2022 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following samples: Laboratory ID Client ID 576962001 MW-31 04112022 576962002 MW-32_04112022 576962003 MW-02 04122022 576962004 MW-25 04122022 576962005 MW-27 04122022 576962006 MW-35 04122022 576962007 MW-18 04132022 576962008 MW-19 04132022 576962009 MW-01 04142022 576962010 MW-29 04142022 576962011 MW-65 04142022 Case Narrative: Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. Page 3 of 25 SDG: 576962 The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Page 4 of25 SDG: 576962 Julie Robinson Project Manager 5 7&0lo ;;J_ I I (" '(?£ Sheet 1 of 1 1· ~ r_ ~ERGYFUELSRESOURCES C ~HAIN OF CUSTODY Samples Shipped to: GELL ~boratories, LLC Contact: Tanner Hollida;z:'. 2040 ~ avage Road Ph: 435 678 2221 Charle ston, SC 29407 tholliday(@,ener9l£fuels.co111 (843} t 56 8171 Chai n of Custody/Sampling Analysis Request Project Samplers Name Samplers Signature 02 Ground Water 2022 Tanner Hollidav ba~MH" »~~ ti Time Sample ID Date C ollected Collected Laboratorv Analvsis Requested MW-31 04112022 4 11/2022 1345 Gross Alpha MW-32 04112022 4 11/2022 1245 Gross Aloha MW-02 04122022 4 12/2022 1335 Gross Alpha MW-25 04122022 4, 12/2022 1055 Gross Aloha MW-27 04122022 4, 12/2022 1115 Gross Alpha MW-35 04122022 4., 12/2022 1420 Gross Alpha MW-18 04132022 4 13/2022 1135 Gross Aloha MW-19 04132022 4 13/2022 1335 Gross Alpha MW-01 04142022 4 14/2022 945 Gross Aloha MW-29 04142022 4, 14/2022 1005 Gross Alpha MW-65 04142022 4, 14/2022 1005 Gross Aloha Comments: Please send report tc Kathv Weinel at kweinel@energvfuels.com Relinquished By:(Signature) Date/Time ReceiMre) Date/Time ~\r,~_ ... ,,, J#'t/f4,ann'er 4/14/2022 ~(/ -~/[({/t ~I Holliday 1100 Relinquished By:(Signa~) Datefrime Reta".. .......... , :t Signature) Date/Time Page 5 of25 SDG: 576962 B j L.alJorntmies uc :s SAMPLE RECEII>'f & REVIEW FORM .. ,..._.._,_ Ji,, t\ , Ciicnt: LJ\\} \\/L \_ SDG/AR/COC/Wotk Order: ~7( ,.,&j(,-,~ Received By:DC .Dllte RC(clvcd: .. \.\--\01 .-'7 "J FedEx Express FedEx Ground~~~cld Services Courier Other Carrier llDd Tracking Number ri \ro+YY1 1"2 q··z. SL {iio bj ·1 Suspected H8.7Jlnl Information l'l Q *If Net Counts> IOOcpm on samples not marked "radioactive", conlact lhe Radiation Safety Group for further investigation. I>< z ·v Hazard Closs Shipped: UN#: A)ShiPDCd as a DOI" Hazardous? If UN2910, Is lhe Radioactive Shipment Survey Compliant? Yes_ No_ B) Did the client designate the samples are lo be ,~ COC notation or radioactive sticken on containers equal ctieni designation. received as radioactive? II" -~ C) Did the RSO classify the samples as X tadiooctive7 "Maximum Net Counts Observed* (Observed Counts -Area Background Counts~ CPM I mR/Hr ,-Clas.sified ns: Rad l Rad 2 Rad 3' D) Did Lbe client designate samples are hazardous? lX rOC notation or-hazard labels on containers equal client designation. 'r,( lf Dor Eis yes, select Hazards below. E) Did the RSO identify possible ha,.ard.s? PCB's Flammable Foreign Soil RCRA Asbestos Beryllium Other. Sample Receipt Criteria ~ < Q / Comments/Qualifiers (Required for Non-Conronning Items) z z Shipping containers received intact and ;!!-~le Applicable: Seals broken Damaged contnincr Leaking container Olher (describe) 1 sealed? Chain of custody documents included /Applicable: Client contacted and provided COC COC created upon receipt : 2 wilh shipment? ~ Preservation Method: Wet Ice Ice Packs Dry i~ther: \G(O 3 Samples requiring cold preservation V ,,-*all lemperalures are recorded in Celsius TEMP: wilhin CO< 6 den. C)?• / Daily check performed and passed on IR , ~faturc Device Serial#: IR2·22 4 temperature gun? dary Temper.tun: Device Serini tt (If Applic:uble): ~ Cirole Applicoblc: Sc•I< broken Dzzmo..£,cd container LcM<lng container Olhcr (cic,cnl>c) s Sample containers intact and sealed? [\ ~ . Samples requiring chemical preservation Somple ID's and Conminers Affected: 6 at proper pH? 1, If Preservation added, Lot#o Ir Yes, are Eno,.ms or Soil Kits pn:sc-.1 for solids? Yes No NA.._(Jryes, toke to VOA Freezer) Do any samples require Volatile Do liquicy.'l)A vials contain acid pre3arvation? Yes No NA_(lrunkl)qwn, select No) 7 Analysis? L~dVOAvi3lsli-ceofheadspace?Yes_ No_ NA_ ,nplc ID'• and containm i!Tccted: ./ 8 Samples received within holding time? ( ~d tests affected: r / ? Sample !D's on COC match ID's on vd containers affected: !,ottles? "" / Date & time on COC match date & time C" le Applicable: No deies on containers No times on container.. COC missing info Other (describe) 10 on bottles? .... / Number of containers received match Circle Appiicablc: No conwiocrcount on COC Other (describe) 11 number indicated on COC? .... / 12 Are sample co.ntairn:rs identifiable as \. GEL Drovidcd bv use of GEL labels? t 13 COC form is properly signed in Circle Applicable: Not relinquished Olher (describe) relinquished/received sections? Comments (Use Continuation Fonn if needed): j I PM(orPMA) riview: Initials \\ l ·1 /)v-Dute v i I .JJJ I;;;). Page __l_ of __ ! GL-CHL-SR-001 Rev 7 Page 6 of25 SDG: 576962 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 576962 Client SDG: 576962 Q2 Ground Water 2022 Project Manager: Project Name: Purchase Order: Package Level: EDD Format: Julie Robinson DNMI00100 White Mesa Mill GW DW16138 LEVEL3 EIM_DNMI GELID Client Sample ID Client Sample Desc. 576962001 MW-31_04112022 576962002 MW-32_04112022 576962003 MW-02_ 04122022 576962004 MW-25_04122022 576962005 MW-27 _04122022 576962006 MW-35_04122022 576962007 MW-18_04132022 576962008 MW-19_04132022 576962009 MW-01 _ 04142022 576962010 MW-29 _04142022 576962011 MW-65_04142022 Client Sample ID Status Tests/Methods -001 MVV-31_04112022 REVVV GFPC, Total Alpha Radium, liquid -002 MVV-32_04112022 REVVV GFPC, Total Alpha Radium, liquid -003 MVV-02_04122022 REVVV GFPC, Total Alpha Radium, liquid -004 MVV-25_04122022 REVVV GFPC, Total Alpha Radium, liquid -005 MVV-27_04122022 REVVV GFPC, Total Alpha Radium, liquid -006 MVV-35_04122022 REVVV GFPC, Total Alpha Radium, liquid -007 MVV-18_04132022 REVVV GFPC, Total Alpha Radium, liquid -008 MVV-19_04132022 REVVV GFPC, Total Alpha Radium, Liquid -009 MVV-01_04142022 REVVV GFPC, Total Alpha Radium, Liquid -010 MVV-29_04142022 REVVV GFPC, Total Alpha Radium, Liquid -011 MVV-65_04142022 REVVV GFPC, Total Alpha Radium, liquid Collect Date& Time 11-APR-22 13:45 11-APR-22 12:45 12-APR-22 13:35 12-APR-22 10:55 12-APR-22 11 :15 12-APR-22 14:20 13-APR-22 11 :35 13-APR-22 13:35 14-APR-22 09:45 14-APR-22 10:05 14-APR-22 10:05 Product Reference Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Work Order Due Date: 17-MA Y-22 Package Due Date: 17-MAY-22 EDD Due Date: Due Date: NG1 Receive Time # of Date& Time Zone Cont. 19-APR-22 10:00 -2 1 19-APR-22 10:00 -2 1 19-APR-22 10:00 -2 1 19-APR-22 10:00 -2 1 19-APR-22 10:00 -2 1 19-APR-22 10:00 -2 1 19-APR-22 10:00 -2 1 19-APR-22 10:00 -2 1 19-APR-22 10:00 -2 1 19-APR-22 10:00 -2 1 19-APR-22 10:00 -2 1 Fax Date PM Comments 17-MAY-22 17-MAY-22 Lab Matrix GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER Report Date: 16-MAY-22 Work Order: 576962 Page 1 of 2 Collector: C Prelogin #: 20190487484 Project Workdef ID: 1294356 SDG Status: Closed Logged by: Fax Days to Prelog Lab Field Due Date Process CofC# 20 20 20 20 20 20 20 20 20 20 20 Aux Data Group QC QC Receive Codes N \0 O'I \0 r--lf) d Q r/). If) N t+-< r-- Q) bJj ro 0,.., GEL Laboratories LLC -Login Review Report Product: GFCTORAL Workdef ID: 1458614 In Product Group? No Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Samples: 001,002,003, 004,005,006, 007,008,009,010, 011 Parmname Check: All parmnames scheduled properly CAS# Contingent Tests Parmname Gross Radium Alpha Action Product Name login Requirements: Requirement Description Group Name: Group Reference: Report Date: 16-MAY-22 Work Order: 576962 Page 2 of 2 Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Client RDL or PQL & Unit Reporting Parm Included Included Custom Units Function in Sample? in QC? list? pCi/L REG y y No Samples Include? Comments Peer Review by: ___________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? _____ _ N I.O 0\ I.O r- lr) c.:, 0 r./J. lr) N <+,.; 0 00 (U ~ 0... Radiochemistry Technical Case Narrative Energy Fuels Resources SDG #: 576962 Product: GFPC, Total Alpha Radium, Liquid Analytical Method: EPA 903.0 Analytical Procedure: GL-RAD-A-044 REV# 10 Analytical Batch: 2261341 The following samples were analyzed using the above methods and analytical procedure(s). Client Sample Identification MW-31 04112022 MW-32 04112022 MW-02 04122022 MW-25 04122022 MW-27 04122022 MW-35 04122022 MW-18 04132022 MW-19 04132022 MW-01 04142022 MW-29 04142022 MW-65 04142022 Method Blank (MB) GEL Sample ID# 576962001 576962002 576962003 576962004 576962005 576962006 576962007 576962008 576962009 576962010 576962011 1205081991 1205081992 1205081993 !205081994 1205081995 57696200l(MW-31_04112022) Sample Duplicate (DUP) 57696200l(MW-31_04112022) Matrix Spike (MS) 57696200l(MW-31_04112022) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (OC) Information Matrix Spike (MS) Recovery Matrix Spike Duplicate did not meet the recovery requirement; however the Matrix Spike did meet the recovery requirement. The Matrix Spike and Matrix Spike Duplicate also meet the relative percent difference requirement. Sample Analyte Value 1205081994 (MW-3 l _ 04 l 12022MSD) Gross Radium Alpha 70.5* (75%-125%) Miscellaneous Information Additional Comments The matrix spike and matrix spike duplicate, 1205081993 (MW-3 l _ 04 l 12022MS) and 1205081994 Page 10 of25 SDG: 576962 (MW-31 _ 04112022MSD), aliquots were reduced to conserve sample volume. Certification tatement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 11 of 25 SDG: 576962 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMI001 Energy Fuels Resources (USA), Inc. Client SDG: 576962 GEL Work Order: 576962 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. Review/Validation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: j~ ~ Name: Theresa Austin Date: 13 MAY 2022 Title: Group Leader Page 12 of25 SDG: 576962 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summarx Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Contact: Ms. Kathy Weinel Workorder: 576962 ------Parmname NOM Unit!...____!!PD% Rad Gas Flow 3atch 2261341 QCI20508l992 576962001 DUP Gross Radium Alpha u 0.595 u Uncertainty +l-0.294 QC1205081995 LCS Gross Radium Alpha 520 Uncertainty QC120508l991 MB Gross Radium Alpha u Uncertainty QC1205081993 576962001 MS Gross Radium Alpha 2190 u 0.595 Uncertainty +l-0.294 QC1205081994 576962001 MSD Gross Radium Alpha 2190 u 0.595 Uncertainty +l-0.294 Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product 0.950 pCilL NIA +l-0.331 425 pCilL +l-5.62 0.392 pCilL +l-0.231 1670 pCilL +l-22.4 1550 pCilL 7.88 +l-22.2 A B BD C D F H K L M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GCIMS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Page 24 of25 SDG: 576962 Reoort Date: May 13, 2022 Page 1 of REC% Ran e Anlst Date Time ---- NIA JXC9 05110122 17:3 81.8 (75%-125%) 05110122 17:3 05/10122 17:3 76.6 (75%-125%) 05/10122 17:3 70.5* (Oo/o-20%) 05110122 17:3 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 576962 Parm name NOM C Units RPO% REC% Ran e Anlst ---- M Matrix Related Failure NIA RPD or %Recovery limits do not apply. NI ND NJ Q R u UI UJ UL X y I\ h See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of Date Time NI A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. /\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where the duplicate value is less than 5X the RL, a control limit of +I-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 25 of 25 SDG: 576962 fflij11 I Laboratories LLC a member of The GEL Group INC PO Box 30712 Charleston.SC29417 2040 Smge Road Charleston. SC 29407 P 84; 556.8171 F 843 766.1 f 78 May 23, 2022 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: White Mesa Mill GW Work Order: 577764 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on April 26, 2022. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies of GEL' s accreditations and certifications can be found on our website at www .gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DW16138 Enclosures Sincerely, Julie Robinson Project Manager gel.com May 23, 2022 Laboratory Identification; GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 577764 Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on April 26, 2022 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. The container for MW-26_04202022 was received out of pH and the client said they would recollect. Sample Identification: The laboratory received the following samples: Laboratory ID Client ID 577764001 MW-05 04182022 577764002 MW-I I 04182022 577764003 MW-14 04182022 577764004 MW-17 04182022 577764005 MW-12 04192022 577764006 MW-15 04192022 577764007 MW-28 04192022 577764008 MW-40 04192022 577764009 MW-26 04202022 577764010 MW-30 04202022 577764011 MW-39 04202022 577764012 MW-36 04212022 577764013 MW-70_04212022 Case Narrative; Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. Page 3 of 27 SDG: 577764 The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Page 4 of27 SDG: 577764 Julie Robinson Project Manager c/e~-.£ I Sheet 1 of 1 <--r. I rr.,1 J/ I' ENERGY FUELS RESOURCES <~HAIN OF CUSTODY Samples Shipped to: GEL L :1boratories, LLC 2040 ~ avage Road Contact: Tanner Holliday Ph: 435 678 2221 Charle~ton, SC 29407 tholliday@energyf uels.com (843H 56 8171 Chai, 1 of Custody/Sampling Analysis Request Project Q2 Ground Water 2022 Sample ID Date C1 >llected MW-05 04182022 4/ 8/2022 MW-11 04182022 4/ 8/2022 MW-14 04182022 4/ 8/2022 MW~17 04182022 4/ 8/2022 MW-12 04192022 4/ 9/2022 MW-15 04192022 4/ 9/2022 MW-28 04192022 4/' 9/2022 MW-40_ 04192022 4/' 9/2022 MW-26 04202022 4/: 0/2022 MW-30 04202022 4/~0/2022 MW-39 04202022 4/: 0/2022 MW-36 04212022 4/~ 1/2022 MW-70 04212022 4/21/2022 Samplers Name Tanner Holliday Time Collected 1500 1120 1500 1155 925 1045 1445 1350 1400 1140 1100 740 740 • Sampfer.5_Signatur~ ,,,. 4=J)~rW4r Laboratorv Analysis Requested Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Comments: Please send report to l,athy Weinel at kweinel@eneravfuels.com ~nquished j]i/J"~e) ().iL(I,//(_,"' ~ ~ .t:franner I-olliday Date/Time Received By:(Signature) 4/21/2022 ~ - 1100 // /C ___., Date/Time __ / uf(Jt{l ~~ Relinquished By:(Signature) Date/Time ;:=:ved By:(Signature) Date/Time Page 5 of 27 SDG: 577764 rm,! Labornto1·\es 11.c I SAMPLE RECEIPT & REVIEW FORM Client: I JA)/\1'L. SDG/AIUCOC/Wurk Oc1kr: '177 7/oL/ Rccci vcd D v: BE D11tc Received: 4.,2,t;-~ Fed Ex Express c,~1<, FedEx Ground UP Field Services Courier Other Carrier and Tracking Number 1-:;i J'il+ Y4~ IJ.. q,~05?' 96'/ Sus11cctcd Hazard lnrormalion ti Q •1f Net Counts> 100:pan on samples nol m1U'kcU "mdiom.:livc", cont.uL1 lhc Rc11.fo.nion Safoty Gmup for further in\'e~tigalion. > :z \ I l11Znrd CJ;sss SJtippcd: UN#; A)Shinn.•d :u • DOT Haz:Jl\luus'! If UN2910, Is the Radioactive Shipmclll Survey Compliant"! Yes_ No_ !l) Dill the clielll designate the smnplcs arc l<J h< \ COC no1atinn orrndiottcti\·e slickcr.i on container.,; equ:11 i:licnl designation. 1-ec"Civcd "' md!noc1ivc'! C) Did the RSO clo.ssify the samples a.s \ Maxin,um Ncl Counts Obscn•cd• (Observed Couuts • Arca Background Counts): ~mlt/Hr nKlionctivc'! CJnssilied a~: Rad I Rud 2 R:id 3 \ COC noration or hazard labels on conlaincr,; equal client dcsignalion. D) DiJ lhc client de<ic11nic <nmnks urc haiard Uil.f] l(D or Eis yes, sclcC1 HMarcl. bdow. E) Di~ the RSO idcn1irv no~s!hlc h:001r~s? \.. PCB's Fl~nm,able Foreign Soil RCRA Asbestos Beryllium Olhcr: Sample Receipt Crilcrin ~ < 0 Cumnrcnts/Quallnena (Required for Non-Confonuing llcms) > z z Shipping containers received intact a, d Cin:lo Applic;obltl s.:~I.J: brukcn D:un:at~\J cm11:1iucr Lcnl.in, cont=aincr 01hcr (~e«ribc) 1 scaled? \ 2 Chain of custody documents included ' Ci,cl< Ar11Jicobl<: CI\C'rn cnn1;1cri:d Qntl pr<wid~d COC COC cr~ah:d upon rcccff'1, with ~hipmcnt'! ·-Pn::.'icrvrniun Method: \Vi:1 kc l<X p,.,ks 01yii.:~ ~ Other: ~~ 3 Sainp!cs requiring cold prcscrl'ation \ "aJI t.:mpcr.uurcs ;u·c: rccor<lcU in Celsius TEMP: within (0 < 6 dee. en• Daily check performed and passed 01 lR Tcmpc'mlurc Device Serial#: !R2-?. I 4 tcrllp~rni ure gu 11? v Sccond:uy Tempcrn1urc Device Serial # (If Applicoblc): C"ircl< Applioahto: s.,,1, 1,,nkon D,11m1Jcd c:on1a,U1cr L!tikin~ cnniaincr Ooh" (do.crihc> s Sample containers intact and scale,t? \ Sam11lc~ requiring chemical prescrva ion \ S;,mptc fl>'$ .nnd Can1~lncr, Affected: Mc;J-~~ 6 at proper pH? lfP1i!.sen":11i1m:hli.Jc<l. l.01Jf: If Yes, arc Eoccre,, or Soil Kits present for solids? Ye.~ No NA_(lfyes. wke 10 VOA Fn:<>cr) Do any samples require Volatile Do li<111id VOA vials rontuin acid pre.<crv-Jlioo? Yes No NA (lfunkuown, select No) 7 Anal)'sis? \ Arc li11uid VOA viols free ofl,catlsp;,t'C? Yes_ No_ NA_ Sample ID's and cont~iincn: afkc1cd: \ IO's and lcsts urrcctcd: 8 Sumplcs received within holding tin •? Sample !D's on COC match !D's on '\ 10·~ unJ et.1n1 Uner.,c :1ffcc:t~,l! !) bolllcs? Date & time on COC match date & imc Circle Applicnbh:: No dales on conlainers No 1imes on conc.iincn. COC miss in~ info Olher (de.scribe) 10 on bottles? ' Number of containers received null, 1 '\ Circle A11plicnbk: N(' conrnincr count on COC Other {dc.'<ribc.) 11 number indicated on COC'/ 12 Are !<:llllple containers id~n1iliablc. · '\ 01:,L provided bv use or GEL lnbcl ? 13 COC form is properly sign~d in ' Cin:lc Applicahle: N,~ n:linc1ul~ticu Ocher (,k,crih,:J rclinquishcd/rcccivcd 11ec1ions'/ Cumments (Use Cuntinuatiun Fonn ifnecJoU): I PM (o rPMA) review: lnitinls \\l'"\Llr: Date L-117, l.:J,'J Page __J_ of L GL·CHL·SR-001 Rev 7 Page 6 of27 SDG: 577764 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 577764 Client SDG: 577764 Q2 Ground Water 2022 Project Manager: Project Name: Purchase Order: Package Level: EDD Format: Julie Robinson DNMI00100 White Mesa Mill GW DW16138 LEVEL3 EIM_DNMI GELID Client Sample ID Client Sample Desc. 577764001 MW-05 _ 04182022 577764002 MW-11_04182022 577764003 MW-14_04182022 577764004 MW-17 _04182022 577764005 MW-12_04192022 577764006 MW-15_04192022 577764007 MW-28_04192022 577764008 MW-40 _ 04192022 577764009 MW-26_04202022 577764010 MW-30_04202022 577764011 MW-39_04202022 577764012 MW-36_04212022 577764013 MW-70_04212022 Client Sample ID Status Tests/Methods -001 MW-05_04182022 REVW GFPC, Total Alpha Radium, Liquid -002 MW-11_04182022 REVW GFPC, Total Alpha Radium, Liquid -003 MW-14_04182022 REVW GFPC, Total Alpha Radium, Liquid -004 MW-17_04182022 REVW GFPC, Total Alpha Radium, Liquid -005 MW-12_04192022 REVW GFPC, Total Alpha Radium, Liquid -006 MW-15_04192022 REVW GFPC, Total Alpha Radium, Liquid -007 MW-28_04192022 REVW GFPC, Total Alpha Radium, Liquid -008 MW-40_04192022 REVW GFPC, Total Alpha Radium, Liquid -009 MW-26_04202022 -010 MW-30_04202022 REVW GFPC, Total Alpha Radium, Liquid -011 MW-39_04202022 REVW GFPC, Total Alpha Radium, Liquid Collect Date & Time 18-APR-22 15:00 18-APR-22 11 :20 18-APR-22 15:00 18-APR-22 11 :55 19-APR-22 09:25 19-APR-22 10:45 19-APR-22 14:45 19-APR-22 13:50 20-APR-22 14:00 20-APR-22 11:40 20-APR-22 11 :00 21-APR-22 07:40 21-APR-22 07:40 Product Reference Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Work Order Due Date: 24-MAY-22 Package Due Date: EDD Due Date: Due Date: NG1 Receive Time # of Date & Time Zone Cont. 26-APR-22 10:05 -2 1 26-APR-22 10:05 -2 , 26-APR-22 10:05 -2 1 26-APR-22 10:05 -2 1 26-APR-22 10:05 -2 1 26-APR-22 10:05 -2 1 26-APR-22 10:05 -2 1 26-APR-22 10:05 -2 1 26-APR-22 10:05 -2 1 26-APR-22 10:05 -2 1 26-APR-22 10:05 -2 1 26-APR-22 10:05 -2 1 26-APR-22 10:05 -2 1 Fax Date PM Comments 24-MAY-22 24-MAY-22 24-MAY-22 Lab Matrix GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER Report Date: 23-MAY-22 Work Order: 577764 Page 1 of 2 Collector: C Prelogin #: 20190487484 Project Workdef ID: 1294356 SDG Status: Closed Logged by: Fax Days to Prelog Lab Field Due Date Process Cote# 20 20 20 20 20 20 20 20 20 20 20 20 20 Aux Data Group QC QC Receive Codes -.::t" \D r--r--r-- V) c., 0 r/). r-- 01 4-< 0 r-- (1.) ~ P-. GEL Laboratories LLC -Login Review Report -012 MW-36_04212022 -013 MW-70_04212022 REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid Product: GFCTORAL Workdef ID: 1458614 Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Gross Alpha Gross Alpha In Product Group? No Samples: 001, 002, 003, 004, 005, 006, 007, 008, 010, 011, 012, 013 Parmname Check: All parmnames scheduled properly CAS# Contingent Tests Parmname Gross Radium Alpha Action Product Name Login Requirements: Requirement Description Group Name: Group Reference: Report Date: 23-MAY-22 Work Order: 577764 Page 2 of 2 Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Client RDL or PQL & Unit Reporting Parm Included Included Custom Units Function in Sample? in QC? List? pCi/L REG y y No Samples Include? Comments Peer Review by:. ___________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? _____ _ -.::t" \0 r-... r-... r-... V) 0 Q r./). r-... N 4-< 0 00 Q) ~ p... Nina Gampe From: Sent: Kathy Weinel <KWeinel@energyfuels.com> Tuesday, April 26, 2022 1 :09 PM To: Nina Gampe; N. Tanner Holliday Cc: Team Robinson Subject: RE: Q2 Ground Water 2022 [EXTERNAL EMAIL) 00 N0li C::~LC~ links or,a~t~ol"lments unle-ss yo·u recognize the senqer and know the content Is safe. Nina, Please dispose of the sample. We will recollect and send a new sample. Thanks Kathy 0 ~ Energy Fuels Resources (USA) Inc. Kathy Weinel Director, Regulatory Compliance t:303.389.4134 I c: I f:303.389.4125 KWeinel@energyfuels.com 225 Union Blvd., Suite 600 Lakewood, CO 80228 http://www.energyfuels.com This e-mail is intended for the exclusive use of person(s) mentioned as the recipient(s). This message and any attached files with it are confidential and may contain privileged or proprietary information. If you are not the intended recipient(s) please delete this message and notify the sender. You may not use, distribute print or copy this message if you are not the intended recipient(s). From: Nina Gampe <Nina.Gampe@gel.com> Sent: Tuesday, April 26, 2022 11:07 AM To: Kathy Weinel <KWeinel@energyfuels.com> Cc: Team Robinson <Team.Robinson@gel.com> Subject: Q2 Ground Water 2022 Good Afternoon, The container for MW-26_04202022 was received with pH>2. Please advise . Thank you, Nina Gampe Project Manager Assistant 1 Page 9 of27 SDG: 577764 ----- GEL Laboratories LLC 2040 Savage Road, Charleston, SC 29407 I P.O. Box 30712, Charleston, SC 29417 Office Main: 843.556.8171 I Office Direct: 843.556.8171 ext. 4778 I Office Fax: 843.769.7383 E-Mail: nina.gampe@gel.com I Website: www.gel.com CONFIDENTIALITY NOTICE: This e-mail and any files transmitted with it are the property of The GEL Group, Inc. and its affiliates. All rights, including without limitation copyright, are reserved. The proprietary information contained in this e-mail message, and any files transmitted with it, is intended for the use of the recipient(s) named above. If the reader of this e-mail is not the intended recipient, you are hereby notified that you have received this e-mail in error and that any review, distribution or copying of this e-mail or any files transmitted with it is strictly prohibited. If you have received this e-mail in error, please notify the sender immediately and delete the original message and any files transmitted. The unauthorized use of this e-mail or any files transmitted with it is prohibited and disclaimed by The GEL Group, Inc. and its affiliates .. Disclaimer The information contained in this communication from the sender is confidential. It is intended solely for use by the recipient and others authorized to receive it. If you are not the recipient, you are hereby notified that any disclosure, copying, distribution or taking action in relation of the contents of this information is strictly prohibited and may be unlawful. This email has been scanned for viruses and malware, and may have been automatically archived by Mimecast, a leader in email security and cyber resilience. Mimecast integrates email defenses with brand protection, security awareness training, web security, compliance and other essential capabilities. Mimecast helps protect large and small organizations from malicious activity, human error and technology failure; and to lead the movement toward building a more resilient world. To find out more, visit our website. 2 Page 10 of27 SDG: 577764 Radiochemistry Technical Case Narrative Energy Fuels Resources SDG #: 577764 Product: GFPC, Total Alpha Radium, Liquid Analytical Method: EPA 903.0 Analytical Procedure: GL-RAD-A-044 REV# 10 Analytical Batch: 2265414 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 577764001 577764002 577764003 577764004 577764005 577764006 577764007 577764008 577764010 577764011 577764012 577764013 1205090715 1205090716 1205090717 1205090718 1205090719 Client Sample ldentification MW-05 04182022 MW-11 04182022 MW-14 04182022 MW-17 04182022 MW-12 04192022 MW-15 04192022 MW-28 04192022 MW-40 04192022 MW-30 04202022 MW-39 04202022 MW-36_04212022 MW-70 04212022 Method Blank (MB) 57776400l(MW-05_04182022) Sample Duplicate (DUP) 57776400l(MW-05_04182022) Matrix Spike (MS) 57776400l(MW-05_04182022) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Miscellaneous Information Additional Comments The matrix spike and matrix spike duplicate, 1205090717 (MW-05 _ 04 l 82022MS) and 1205090718 (MW-05_04182022MSD), aliquots were reduced to conserve sample volume. Certification tatement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 12 of27 SDG: 577764 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMI001 Energy Fuels Resources (USA), Inc. Client SDG: 577764 GEL Work Order: 577764 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. Review/Validation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: j~ ~ Name: Theresa Austin Date: 23 MAY 2022 Title: Group Leader Page 13 of 27 SDG: 577764 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Contact: Workorder: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Ms. Kathy Weinel 577764 Parm name Rad Gas Flow NOM=-----=S-=a=m le Q_ual 3atch 2265414 QC1205090716 577764001 DUP Gross Radium Alpha QC 1205090719 LCS Gross Radium Alpha QC1205090715 MB Gross Radium Alpha QCl205090717 577764001 MS Gross Radium Alpha QC1205090718 577764001 MSD Gross Radium Alpha Notes: u Uncertainty 533 Uncertainty Uncertainty 2130 U Uncertainty 2150 U Uncertainty 0.0181 U +/-0.139 0.0181 +/-0.139 0.0181 +/-0.139 u Counting Uncertainty is calculated at the 68% confidence level (I-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product _QC 0.248 +/-0.216 517 +/-5.74 0.0335 +/-0.233 1640 +/-20.1 1720 +/-20.4 Units pCi/L pCi/L pCi/L pCi/L pCi/L RPD% NIA 5.2 A B BD C D F H K L M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Page 26 of 27 SDG: 577764 Reoort Date: May 23, 2022 Page 1 of REC% Ran e Anlst Date Time NIA JXC9 05/18122 13:1 97 (75%-125%) 05/18122 13:1· 05/18122 13 :1· 77 (75%-125%) 05118122 13:1 80.1 (0%-20%) 05/18122 13:1 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 577764 Page 2 of Parmname NOM Samp!!__.._u-'-al'--_ QC Units RPO% REC% Ran e Anlst Date Time M Matrix Related Failure NIA RPO or %Recovery limits do not apply. NJ ND NJ Q R u UJ UJ UL X y See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound ----- /\ h RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. "The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where the duplicate value is less than 5X the RL, a control limit of +I-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 27 of 27 SDG: 577764 (iJij! Laboratories LLC a member of The GEL Group INC PO Box :l0712 Chan eston. SC 2941 7 2040 Savage Road Charleston. SC 29407 P 84~ 556.8171 F 843.766 117S June O 1, 2022 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: White Mesa Mill G W Work Order: 578558 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on May 03, 2022. This revised data report has been prepared and reviewed in accordance with GEL's standard operating procedures. This package was revised to correct the date on the letter. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DW16138 Enclosures Sincerely, Julie Robinson Project Manager lll BIIIIIIUI 11111111 U I.I I gel.com This package was revised to correct the date on the letter. June 01, 2022 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 578558 Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on May 03, 2022 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following samples: Labgratory ID Client ID 578558001 M\ll-22 042520222 578558002 M\ll-03A 04272022 578558003 M\ll-23 04272022 578558004 M\ll-24 04272022 578558005 M\ll-24A 04272022 578558006 M\ll-38 04272022 578558007 T\l/4-24_04272022 578558008 M\ll-26 04272022 Case Narrative: Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. Page 3 of 22 SDG: 578558 Revl The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Page 4 of22 SDG: 578558 Revl Julie Robinson Project Manager 57%'5S8 /,.-' . .r.l (·,~~,'} ~.J ENERGYFUELSRESOURCES Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: _G_E_L_L_a_bo_r_at_o_rie_s .... , _L_LC _______ Contact: Tanner Holliday 2040 Savage Road Ph: 435 678 2221 Charleston, SC 29407 tholliday@enerqyfuels.com (843) 556 8171 Chain of Custody/Sampling Analysis Request Project Samplers Name Samplers Signa,tu,e 02 Ground Water 2022 Tanner Holliday L ~,1,,;;,~ -Q-4__, ~ , Time Sample ID Date Collected Collected Laboratorv Analysis Requested MW-22 042520222 4/25/2022 1250 Gross Alpha MW-03A 04272022 4/27/2022 915 Gross Alpha MW-23 04272022 4/27/2022 840 Gross Alpha MW-24 04272022 4/27/2022 800 Gross Alpha MW-24A 04272022 4/27/2022 740 Gross Alpha MW-38 _ 04272022 4/27/2022 1030 Gross Alpha TW4-24 04272022 4/27/2022 1230 Gross Alpha MW-26 04272022 4/27/2022 945 Gross Alpha Comments: Please send report to Kathy Weinel aj kweinelc@energyfuels.com ~ Relinquished By:(Si~:t'~ Date/Time Received By:(Signature) __ Date/T~ 4/28/2022 ~-~ ,..~ . ...< .:-),.. ,,.,.,,,~,.,, ff ~anner Holliday 1100 ~· \t\S ') Relinquished By:(Signature) Date/Time Re~:(Signature) Date/Time Page 5 of 22 SDG: 578558 Revl 831 / Latmatones i. LC Client: Received B Carrier and Tracking Number S1Lspcclcd Haznrd Information AlShi •d as a DOT Hawnlous0 8) Did lhe client Jcsiynale the samples are to he received n.'i rndioactivc? C) Did the RSO cla.ssi fy the samples a.s ra<lioaclivc? D) Did lhc clic:nl desi ate smn lcs arc hazardous? I,) Did the RSO identif ,ssihle hazar<ls? Sample Receipt Criteria Shipping containers received intact and scaled? 2 Chain of custody documents included with shipment'/ 3 Samples requiring cold preservation within (0 < 6 de, C)?* 4 Daily check performed and passed on IR temperature gtm? 5 Sample conlainers intact and scaled? 6 Samples requiring chemical preservation at proper pH? 7 Do any samples require Volatile Analysis? Samples received within holding time? Sample ID's on COC match !D's m1 bottles? Date & time on COC malch date & time on bottles? 12 Arc smnple container., identifiable as GEL rovided b use of GEL labels? 13 COC form is properly signed in relinquished/recei vcd sections? Comments (Use Continuation Form if needed): Page 6 of22 SDG: 578558 Revl SAMPLE RECEIPT & REVIEW FORM SDG/AR/COC/Work Order: Date Received: FedEx Express FedEx Ground Courier Other ~ ~ ~If Net Counls > lOOcpm on s;tmplcs 1101 marked ''radiow.:1ive", con1m.:t the Rm..li,,lion Safety Group for fur1hcr invc~aig11tion. \ Hazard Class Shipped: UN#: If UN29t0, Is lhc Radioactive Shipment Survey Compliant? Yes_ No_ ' COC notation or radioactive stickers nn containers eql:lal client des~gnation~ Maximum Net Counts Observed• (Observed Counts -Arca Backpround Counts): , Clossificd as: Rud I Rud 2 Rad 3 '\ CDC nolntion or hnzanl 1.nbcls on containers equal client dciignation. If Dor I, is yes, select Hazards below. PCB's Flammable Foreign Soil RCRA Asbestos Beryllium Other: Commcnts/Qnalilic1-s (Required for Non-Conforming Items) Cirdc Applknble: Seals broken Dumngetl cnnlainer Leaking comaincr 01hcr (describe) Circle A11plicahlc: Clicnl con1ac1cd nnd provided COC Pn,servation Mclho<l: Wet kc Ice Packs Dry ice *ull lcmr,emtm-cs arc recorded in Celsius Temperature Device Serial l/:,~IR~2~-~2~1 ____ _ Secondary TempcrJture Device Serial# (If Applicable): COC created upon rcccipl Olhci: Circle Applic.tt,Jc: Seals hrokcn Damngcd con1ai.ncr Le akin~ con1uincr 01hcr (dc:.crihc) Sample ILYs and Containers Affected: Ir Pr~scrvutinn m.ldcd. Lu1f#: If Yes, are Encores or Soil Kits present ror solids'/ Yes_ No_ NA_(ll'yes. take 10 VOA Freezer) Do lic1uid VOA vials contain add preservation? Yes_ No_ NA_(lfu11known. select No) Are liquid VOA vials free ofheadspacc'/ Yes_ No_ NA_ Sumplc ID's and conlaincrs affcclcd: ID'.s and tests affected: ID's and container.; 11ffectcd: Circle Applicable: No dales on containers No limes on containers COC missing info Other (describe) Circle Applicable: No container count on COC Other (describe) Circle Applicahle: Nol rclin4uish«I 01her (describe] Page __ of GL-CHL-SR-001 Rev 7 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 578558 Q2 Ground Water 2022 ClientSDG: Project Manager: Project Name: Purchase Order: Package Level: EDD Format: 578558 Julie Robinson DNMI00100 White Mesa Mill GW DW16138 LEVEL3 EIM_DNMI GELID Client Sample ID Client Sample Desc. 578558001 MW-22_042520222 578558002 MW-03A_04272022 578558003 MW-23_04272022 578558004 MW-24_04272022 578558005 MW-24A_04272022 578558006 MW-38 _ 04272022 578558007 TW4-24_04272022 578558008 MW-26 _ 04272022 Client Sample ID Status Tests/Methods -001 MVV-22_042520222 REVW GFPC, Total Alpha Radium, Liquid -002 MW-03A_04272022 REVW GFPC, Total Alpha Radium, Liquid -003 MW-23_04272022 REVW GFPC, Total Alpha Radium, Liquid -004 MW-24_04272022 REVW GFPC, Total Alpha Radium, Liquid -005 MW-24A_04272022 REVW GFPC, Total Alpha Radium, Liquid -006 MW-38_04272022 REVW GFPC, Total Alpha Radium, Liquid -007 TW4-24_04272022 REVW GFPC, Total Alpha Radium, Liquid -008 MW-26_04272022 REVW GFPC, Total Alpha Radium, Liquid Collect Date & Time 25-APR-22 12:50 27-APR-22 09:15 27-APR-22 08:40 27-APR-22 08:00 27-APR-22 07:40 27-APR-22 10:30 27-APR-22 12:30 27-APR-22 09:45 Product Reference Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Work Order Due Date: 01-JUN-22 Package Due Date: EDD Due Date: Due Date: NG1 Receive Time # of Date & Time Zone Cont. 03-MAY-22 10:55 -2 1 03-MAY-22 10:55 -2 1 03-MAY-22 10:55 -2 1 03-MAY-22 10:55 -2 1 03-MAY-22 10:55 -2 1 03-MAY-22 10:55 -2 1 03-MAY-22 10:55 -2 1 03-MAY-22 10:55 -2 1 Fax Date PM Comments 01-JUN-22 01-JUN-22 01-JUN-22 Lab Matrix GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER Report Date: 01-JUN-22 Work Order: 578558 Page 1 of 2 Collector: C Prelogin #: 20190487484 Project Workdef ID: 1294356 SDG Status: Closed Logged by: Fax Days to Prelog Lab Field Due Date Process CofC# 20 20 20 20 20 20 20 20 Aux Data Group QC QC Receive Codes -> ~ 00 V") 00 (' V") d 0 C/"l N N ,_ 0 r--- Q) ~ 0.... GEL Laboratories LLC -Login Review Report Product: GFCTORAL Workdef ID: 1458614 Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Samples: 001, 002, 003, 004, 005, 006, 007, 008 Parmname Check: All parmnames scheduled properly CAS# Parmname Gross Radium Alpha In Product Group? No Action Product Name Description Contingent Tests Login Requirements: Requirement Group Name: Group Reference: Report Date: 01-JUN-22 Work Order: 578558 Page 2 of 2 Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Client RDL or PQL& Unit Reporting Parm Included Included Custom Units Function in Sample? in QC? List? pCi/L REG y y No Samples Include? Comments Peer Review by: ___________ _ Work Order (SDG#}, PO# Checked? ____ _ C of C signed in receiver location? _____ _ ...... > ~ 00 tr) tr) 00 r:-- tr) ci Q 17.J N N 4-, 0 00 (l) ~ ~ Radiochemistry Technical Case Narrative Energy Fuels Resources SDG #: 578558 Product: GFPC, Total Alpha Radium, Liquid Analytical Method: EPA 903.0 Analytical Procedure: GL-RAD-A-044 REV# 10 Analytical Batch: 2268525 The following samples were analyzed using the above methods and analytical procedure(s). Client Sample Identification MW-22 042520222 MW-03A 04272022 MW-23 04272022 MW-24 04272022 MW-24A 04272022 MW-38 04272022 TW4-24_04272022 MW-26_04272022 Method Blank (MB) GEL Sample ID# 578558001 578558002 578558003 578558004 578558005 578558006 578558007 578558008 1205096974 1205096975 1205096976 1205096977 1205096978 57855800l(MW-22_042520222) Sample Duplicate (DUP) 57855800l(MW-22_042520222) Matrix Spike (MS) 57855800l(MW-22_042520222) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Preparation Information Homogenous Matrix Sample had light sandy sediment and a sulfur odor. 1205096975 (MW-22_042520222DUP), 1205096976 (MW-22_042520222MS), 1205096977 (MW-22_042520222MSD) and 578558001 (MW-22_042520222). Oualitv Control (QC) Information Matrix Spike (MS) Recovery Matrix spike (See Below) recovery requirement not met due to the matrix of the sample. Sample Analyte Value 1205096976(MW-22_042520222MS) Gross Radium Alpha 51.3* (75%-125%) Matrix Spike Duplicate (See Below) recovery requirement not met due to the matrix of the sample. Page 10 of22 SDG: 578558 Revl Sample Analyte Value 1205096977 (MW-22_042520222MSD) Gross Radium Alpha 58.8* (75%-125%) Miscellaneous Information Additional Comments The matrix spike and matrix spike duplicate, 1205096976 (MW-22_042520222MS) and 1205096977 (MW-22_042520222MSD), aliquots were reduced to conserve sample volume. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 11 of 22 SDG: 578558 Revl GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMIOOI Energy Fuels Resources (USA), Inc. Client SDG: 578558 GEL Work Order: 578558 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. Review/Validation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: j~ ~ Date: 27 MAY 2022 Page 12 of 22 SDG: 578558 Revl Name: Theresa Austin Title: Group Leader GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Workorder: Suite 600 Lakewood, Colorado Ms. Kathy Weinel 578558 Parm name NOM --------------- R. ad Gas Flow 3atch 2268525 QC1205096975 578558001 DUP Gross Radium Alpha QC1205096978 LCS Gross Radium Alpha QC1205096974 MB Gross Radium Alpha QC1205096976 578558001 MS Gross Radium Alpha QC1205096977 578558001 MSD Gross Radium Alpha Notes: Uncertainty 522 Uncertainty Uncertainty 2150 Uncertainty 2070 Uncertainty Sam le 2.05 U +/-0.439 u 2.05 +/-0.439 2.05 +/-0.439 Counting Uncertainty is calculated at the 68% confidence level (I-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product 0.952 +/-0.287 407 +/-5.60 -0.151 +/-0.0878 1100 +/-18.3 1220 +/-19.1 Units pCi/L pCi/L pCi/L pCi/L pCi/L RPO% 73.3 10.2 A B BO C D F H K L M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Page 21 of 22 SDG: 578558 Revl Reoort Date: May 26, 2022 Page I of REC% Ran e Anlst Date Time (0%-100%) JXC9 05/24/22 13:1 78.1 (75%-125%) 05/24/22 13: 1 05/24/22 13:1 51.3* (75%-125%) 05/24/22 13: 1 58.8* (0%-20%) 05/24/22 13:1 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 578558 Parmname NOM Sam le Qual __ Q__C _U=--n=i=ts'--_RPD% REC% Range Anlst M Matrix Related Failure NIA RPD or %Recovery limits do not apply. NI ND NJ Q R u Ul UJ UL X y I\ h See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of Date Time NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPO not applicable. /\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where the duplicate value is less than 5X the RL, a control limit of +I-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 22 of22 SDG: 578558 Revl m=t• I Laboratories LLC a member of The GEL Group INC P0Box30712 ChaMeston.SC29417 204 O Sa•,aoe Road ChaM eston SC 29407 P 84'.:. 556 8171 F 843 76G 1178 June 16, 2022 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: White Mesa Mill GW Work Order: 580437 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on May 19, 2022. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DWI6138 Enclosures Sincerely, Julie Robinson Project Manager gel com June 16, 2022 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 580437 Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on May 19, 2022 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following samples: Case Narrative: Laboratory JD 580437001 580437002 Client ID MW-20 05172022 MW-37_05172022 Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in Jhe analytical case narratives in the enclosed data package. The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the folJowing fractions: Radiochemistry. Page 3 of 15 SDG: 580437 Julie Robinson Project Manager Sheet 1 of 1 >~~~ . f/11,;;'_,-;.~ERGY FUEL S RESOURCES CHAIN OF CUSTODY Samples Shipped to: _G_E_L_L_a_b_or_a_to_ri_e_s, __ L_L_C _______ Contact: Tanner Holliday 2040 Savage Road Ph : 435 678 2221 Charleston, SC 29407 tholliday@energyfuels.com (843) 556 8171 Chain of Custody/Sampling Analysis Request p . roJect s amp ers N ame s amp ers Signature, 02 Ground Water 2022 Tanner Holliday l~~)tttt;/ V Time Sample ID Date Collected Collected Laboratory Analysis ReQuested MW-20 05172022 5/17/2022 800 Gross Alpha MW-37 05172022 5/17/2022 830 Gross Alpha Comments: Please send report to Kathy Weinel at kweinel@enerovfuels.com Date/Time Received ~y:J1ign~~re) 5/17/2022 ~ 1100 Date/Time Received By:(Signature) Page 4 of 15 SDG: 580437 Laboratories LLC SAMP!-E RECEIPT & REVIEW FORM . " ., ' -· Client: d )WrVl l Sl)G/AR/COC/Work Order: s fo43 J " .. . ·-P& c:-hc, I z 2:..... Received By: Onie Rec~!ved: ' .. -~ble: FedEll Express FedEx Groun UPS Field Services Courier Other Carrier anci Tracking Number I} I 0 7 y '1 y' 0 Z..-9S-olJ /t../z..J,- Su.~pectcd Hazunl Information ~ ,£ '!.f Net Counts> IOOcpm on samples not llllllked "radioactive", contact the Radiation Safety Group for further investigation. 'j Hnzru:d Class Shipped: UN#: A)Shinncd :is a DOT H32111'dous'/ IfUN2910, Is the Radioactive Shipment Survey Compliant? Yes_ No_ B) Did the client designate the samples are to be \ COC notation or radio:!Ctive ttickcrs on con1olnars equal client designation. received tlS rndionctive7 ~"'/'"l.L_ C) Did the RSO classify the samples as (X Mrudmum Net Counts Observed• (Observed Counts-Area Background Counts): · Ji, mMlr mdioactive? ·-Cbas.~lfied us: Rad 1 Rad 2 Rad 3 D) Did the clienl dcsil!tlnte samples are hnznrdous? X. COC notD.tlon or hazard labels on contolnon cqunl ollont dcsignotiOtL X IfD or E is yes, select HllZIU'ds below. E) Did the RSO idcntifv oosslble hnznrds? · PCB's Flammable Foreign Soil RCRA Asbestos Beryllium Other. Snmplc Receipt Criteria I.'! < ., Comments/Qualifiers (Required for Non-Conforming Items) > z z Shipping containers received intact and ~ Circle AppHc:abl<:: Seal, b,oken Dam2gcd container Lcakin& container Olher (dc,cnl,o) 1 senlcd? 2 Chain of custody documents included v" Circle Applicablo: Clicnl conu,c1cd ond provided COC COC crcalcd upon receipt with shipmcnt? [>reservation Method: Wet Ice Ice Pncks Dryi~ Other. 3 Samples requiring cold preservation *all temperatures are recorded in Celsius TEMP: z... 3 within (0 < 6 dell. C)?• - Daily check perfonned and passed on IR Tcmpcruture Device Sc.riu!ff: / '"-2 -7--J 4 temperature gun? I>( Second:uy Temperature Device Serial# (If Applicable): ~ Circle Applicoblo: Seals broken Damaged contoincr Ltakinc con1~incr Olher (describe) 5 Sample containers intact and sealed? Samples requiring chemical preservation Sample ID"s •nd Contolnc11 Afrccted: 6 ut proper pH? If Prcscrv:,llon llddcd. Lot/I: IJ Yes, are Encores or Soil Kits present for solids? Yes_ No_ NA..._([f yes, take to VOA Fn:ezcr) Do any samples require Volatile Do liquid VOA vials contain acid prcse,votion7 Yes_ No_ N~(lfunkno"'1l, select No) 7 Analysis? X Arc liquid VOA virus free of hcodspncc7 Yes_ No_ NA.__ Sample ID's and contain«> affccled: . ~ !O's Md tests uffec:tcd: 8 Samples received within holding time? Sample ID's on COC match IO's on ID's and containers ntfected: 9 bottles? X Date & time on COC match date & time Cude Applicable: No runes on conlninors No times on conutincr.. COC missing info Otlicr (describe) 10 on bottles? ~ Number of containers received match r<, Cude AppliCllble: No container count on COC Other (dcsmbc) 11 number indicated on COC? 12 Arc sample containers identifiable as X GEL providc4 by use of GEL labels? 13 COC fonn is ,roperly signed in X Circle Applicnblc: Not n:linguish.cd Other (cl<!scribe) relinquished/received sections? Comments (Use Continuation Form if needed): I I PM (or PMA) review: Initials fiT"\ Date 5 / 'VO 1,, l, Page _i_ of..\...- Page 5 of 15 SDG: 580437 GL-CHL-SR-001 Rev 7 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 580437 Client SDG: 580437 Q2 Ground Water 2022 Work Order Due Date: 17-JUN-22 Package Due Date: 17-JUN-22 Report Date: 16-JUN-22 Work Order: 580437 Page 1 of 2 Collector: C Prelogin #: 20190487484 Project Workdef ID: 1294356 SDG Status: Closed Logged by: Project Manager: Project Name: Purchase Order: Package Level: EDD Fonnat: Julie Robinson DNMI00100 White Mesa Mill GW DW16138 LEVEL3 EIM_DNMI GELID Client Sample ID Client Sample Desc. 580437001 MIIV-20_05172022 580437002 MIIV-37_05172022 Client Sample ID -001 MW-20_05172022 -002 MW-37 _05172022 Status Tests/Methods REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid Collect Date & Time EDD Due Date: Due Date: JAR1 Receive Time # of Date & Time Zone Cont. 17-MAY-22 08:00 19-MAY-22 10:05 -2 17-MAY-22 08:30 19-MAY-22 10:05 -2 Product Reference Gross Alpha Gross Alpha Fax Date PM Comments Product: GFCTORAL Workdef ID: 1458614 In Product Group? No Group Name: Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Samples: 001, 002 Parmname Check: All parmnames scheduled properly CAS# Contingent Tests Parmname Gross Radium Alpha Action Product Name Description Client RDL or PQL & Unit Samples 17-JUN-22 17-JUN-22 Lab Matrix Fax Days to Due Date Process CofC# Prelog Lab Field Group QC QC GROUND IIVATER GROUND IIVATER 20 20 Aux Data Group Reference: Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Reporting Parm Included Included Custom Units Function in Sample? in QC? List? pCi/L REG y y No Receive Codes C') s::t" 0 00 V) ci 0 r::/) V) -4-, 0 \D Login Requirements: Include? Comments o Requirement ~ A.. GEL Laboratories LLC -Login Review Report Peer Review by: ___________ _ Work Order (SDG#), PO# Checked? ____ _ Report Date: 16-JUN-22 Work Order: 580437 Page 2 of 2 C of C signed in receiver location? _____ _ r---M "1" 0 00 tr) tJ Cl rJJ. tr) ...... 4-< 0 r--- (1) ~ i::i... Radiochemistry Technical Case Narrative Energy Fuels Resources SDG #: 580437 Product: GFPC, Total Alpha Radium, Liquid Analytical Method: EPA 903.0 Analytical Procedure: GL-RAD-A-044 REV# 10 Analytical Batch: 2268525 The following samples were analyzed using the above methods and analytical procedure(s). Client Sam pie Identification MW-20 05172022 MW-37 05172022 Method Blank (MB) GEL Sample ID# 580437001 580437002 1205096974 1205096975 1205096976 1205096977 1205096978 57855800l(MW-22_042520222) Sample Duplicate (DUP) 578558001(MW-22_042520222) Matrix Spike (MS) 578558001(MW-22_042520222) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Preparation Information Homogenous Matrix Sample had light sandy sediment and a sulfur odor. 1205096975 (MW-22_042520222DUP), 1205096976 (MW-22_042520222MS) and 1205096977 (MW-22_042520222MSD). Quality Control (QC) Jnformation Matrix Spike (MS) Recovery Matrix spike (See Below) recovery requirement not met due to the matrix of the sample. Sample Analyte Value 1205096976(MW-22_042520222MS) Gross Radium Alpha 51.3* (75%-125%) Matrix Spike Duplicate (See Below) recovery requirement not met due to the matrix of the sample. Sample Analyte Value 1205096977 (MW-22 _ 042520222MSD) Gross Radium Alpha 58.8* (75%-125%) Miscellaneous Information Page 9 of 15 SDG: 580437 Additional Comments The matrix spike and matrix spike duplicate, 1205096976 (MW-22_042520222MS) and 1205096977 (MW-22_042520222MSD), aliquots were reduced to conserve sample volume. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 10 of 15 SDG: 580437 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMI001 Energy Fuels Resources (USA), Inc. Client SDG: 580437 GEL Work Order: 580437 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. Review/Validation GEL requ ires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a th ird level review of the fractional data package. The following data validator verified the information presented in this data report: Signature:~ 6~ Name: Kenshalla Osten Date: 16 JUN 2022 Title: Analyst I Page 11 of 15 SDG: 580437 Contact: Workorder: GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com Energy Fuels Resources (USA), Inc. 225 Union Boulevard QC Summary Reoort Date: June 16, 2022 Suite 600 Lakewood, Colorado Ms. Kathy Weinel 580437 NOM _ _fu!_mp_le Qual __ QC __ Units RPO% REC% Range Anlst Parmname Rad Gas Flow 3atch 2268525 QC 1205096975 578558001 DUP Page 1 of Date Time Gross Radium Alpha 2.05 U 0.952 +/-0.287 pCi/L 73.3 (0%-100%) JXC9 05/24/22 13:1 QC 1205096978 LCS Gross Radium Alpha QC 1205096974 MB Gross Radium Alpha QC 1205096976 578558001 Gross Radium Alpha QC 1205096977 578558001 Gross Radium Alpha Notes: MS MSD Uncertainty 522 Uncertainty Uncertainty 2150 Uncertainty 2070 Uncertainty +/-0.439 u 2.05 +/-0.439 2.05 +/-0.439 Counting Uncertainty is calculated at the 68% confidence level (I-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product 407 +/-5.60 -0.151 +/-0.0878 1100 +/-18.3 1220 +/-19.1 pCi/L pCi/L pCi/L pCi/L 10.2 A B BO C D F H K L M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Page 14 of 15 SDG: 580437 78.1 (75%-125%) 05/24/22 13: I 05/24/22 13:1 51.3 * (75%-125%) 05/24/22 13: I 58.8* (0%-20%) 05/24/22 13:1 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 580437 Parm name NOM Sample Qu_a_l __ Units RPO% REC% ~e Anlst M Matrix Related Failure NIA RPD or %Recovery limits do not apply. Nl ND NJ Q R u UI UJ UL X y A h See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of Date Time NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPO not applicable. A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (SX) the contract required detection limit (RL). In cases where the duplicate value is less than 5X the RL, a control limit of +I-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 15 of 15 SDG: 580437 9632 South 500 West CHEMTECH-FORD LABORATORIES 5/26/2022 Work Order: 22 E 1133 Project: 2nd Quarter Groundwater 2022 Energy Fuels Resources, Inc. Attn: Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Client Service Contact: 801.262.7299 The analyses presented on this report were performed in accordance with the National Environmental Laboratory Accreditation Program (NELAP) unless noted in the comments, flags, or case narrative. If the report is to be used for regulatory compliance, it should be presented in its entirety, and not be altered. Approved By: Melissa Connolly, Project Manager Sandy, Utah 84070 801.262. 7299 Main 866.792.0093 Fax Serving the lntermountain West since 1953 www.ChemtechFord.com CHEM TECH-FORD LABORATORIES Energy Fuels Resources, Inc. Project: 2nd Quarter Groundwater 2022 Project Manager: Tanner Holliday Laboratory ID 22E1133-01 22E1133-02 22E1133-03 22E1133-04 22E1133-05 22E1133-06 22E1133-07 22E1133-08 Sample Name MW-31_04112022 MW-32_04112022 MW-02_04122022 MW-25_04122022 MW-27 _04122022 MW-35_04122022 MW-18_04132022 MW-19_04132022 Work Order Report Narrative Total Dissolved Solids Comments These samples were originally analyzed within the holding time on workorder 220 1197. Due to laboratory error the samples were over-diluted. The analytical results acquired for the Total Dissolved Solids and TDS Ratio have been determined to be inaccurate and biased high as reported on 220 1197. The samples were reanalyzed outside of the holding time and reported on workorder 22E1133. The TDS Ratio reported on 22E1133 was calculated from the TDS analyzed for 22E1133, and the TDS, Calculated from 2201197. Sample Preparation The TDS was prepared outside of method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions The corrective action required with this workorder and the Total Dissolved Solids analysis included additional training on proper sample aliquot and dilutions. Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com CtF WO#: 22E1133 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-31_04112022 Matrix: Water Date Sampled: 4/11/22 13:45 ( all-111:ttion, TDS Ratio lnorl,!anir Total Dissolved Solids (TDS) 1.2 2800 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com None mg/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 5/26/2022 Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting Limit 20 Sampled By: Tanner Holliday SM2340B SM 2540C CtF WO#: 22E1133 Preparation Date/Time 5/5/22 5/10/22 Lab ID: 22El133-01 Analysis Date/Time 5/24/22 5/10/22 APH-R Page 3 of 11 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L460,o\TOll1ES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-02_04122022 Matrix: Water Date Sampled: 4/12122 13:35 ( akulation, TDS Ratio lnort!anil' Total Dissolved Solids (TDS) I.I 3280 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com None mg/L Certificate of Analysis Minimum Reporting Limit 20 PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 5/26/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM2340 B SM2540C CtF WO#: 22E 1133 Preparation Date/Time 5/5/22 5/10/22 Lab ID: 22E1133-03 Analysis Date/Time 5/24/22 5/10/22 APH-R Page 4 of 11 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA80R,HOAIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-25_04122022 Matrix: Water Date Sampled: 4/12/22 10:55 TDS Ratio Total Dissolved Solids (TDS) 1.2 2860 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com None mg/L Certificate of Analysis Minimum Reporting Limit 20 PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 5/26/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM2340 B SM2540C CtF WO#: 22E1133 Preparation Date/Time 5/5/22 5/10/22 Lab ID: 22El133-04 Analysis Date/Time 5/24/22 5/10/22 APH-R Page 5 of 11 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lAD0 e4t011tf.S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-35_04122022 Matrix: Water Date Sampled: 4/12/22 14:20 ( a k11l:1t111n, TDS Ratio lnorl,!allH' Total Dissolved Solids (TDS) I.I 3700 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com None mg/L Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 5/26/2022 Project Name: 2nd Quarter Groundwater 2022 Minimum Reporting Limit 20 Sampled By: Tanner Holliday SM2340B SM2540C CtF WO#: 22E1133 Preparation Date/Time 5/5/22 5/10/22 Lab ID: 22E1133-06 Analysis Date/Time 5/24/22 5/10/22 APH-R Page 6 of 11 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA60RAf0RIE5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-18_04132022 Matrix: Water Date Sampled: 4/13/22 11 :35 ( ,ill'11latiom TDS Ratio lnor~anil· Total Dissolved Solids (TDS) I.I 3090 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com None mg/L Certificate of Analysis Minimum Reporting Limit 20 PO#: Receipt: 4/15/22 16:40@ 0.9 °C Date Reported: 5/26/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM2340 8 SM2540C CtF WO#: 22E1133 Preparation Dale/Time 5/5/22 5/10/22 Lab ID: 22E1133-07 Analysis Date/Time 5/24/22 5/10/22 APH-R Page 7 of 11 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD I AeO•oJ\ JO t1(S Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-19_04132022 Matrix: Water Date Sampled: 4/13/22 13:35 ( akula1i11n, TDS Ratio lnor1!anil' Total Dissolved Solids (TDS) 1.2 1050 Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com None mg/L Certificate of Analysis Minimum Reporting Limit 20 PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 5/26/2022 Project Name: 2nd Quarter Groundwater 2022 Sampled By: Tanner Holliday SM2340B SM2540C CtF WO#: 22E1133 Preparation Date/Time 5/5/22 5/10/22 Lab ID: 22El133-08 Analysis Date/Time 5/24/22 5/10/22 APH-R Page 8 of 11 I CHEMTECH·FORD Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations Certificate of Analysis PO#: Receipt: 4/15/22 16:40@ 0.9 ·c Date Reported: 5/26/2022 Project Name: 2nd Quarter Groundwater 2022 ND= Not detected at the corresponding Minimum Reporting Limit (MRL). 1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = I part per million I ug/L = one microgram per liter or I ug/kg = one microgram per kilogram = I part per billion. I ng/L = one nanogram per liter or l ng/kg = one nanogram per kilogram = I part per trillion. Flag Descriptions APH-R = This sample was originally analyzed within the EPA-recommended holding time. The reported value was obtained from a confirmatory re-analysis that was performed outside of that holding time. Project Name: 2nd Quarter Groundwater 2022 www.ChemtechFord.com CtF WO#: 22E1133 Page 9 of 11 ~) ,v') ,., 03 0~ DJ od Oj og 0"1 · lo -,, American West Analytical Laboratories 463 W. 3600 S. Salt Lake City, VT 84115 Phone# (801) 263-8686 Toti Free# (888) 263-8686 L~ Fax# (801) 263-8687 Email awal@ewel~abs.com www.awal-labs.com Client: Enera:y Fuela Resources, Inc. Address: 6425 S. Rwy. 191 Blanding, UT 84511 Contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: Email: thollidaJ@enerufaela.com.; KWelnel@enerafv.elll.com Project Name: 2nd Quarter Ground water 2022 Project#: PO#: Sampler Name: Tanner Holliday _ _,7' ,,n-, 22E1133 -TDS Only MC 5/13/22 Date C,.~Vrl • l Samole ID: Samoled IIW-31_04112022 4/11/2022 ' -. ........ ------·- IIW-02 04122022 4/12/2022 IIW-25_04122022 4/12/2022 --. ----., ·- MW-3S 04122022 4/12/2022 KW-18 04132022 4/13/2022 IIW-19_04132022 4/13/2022 ---..__ .. -·--·-,_ ,, . . ·-,--··-~-. -·-. ·----· .... _ - J~ , ... ~ »....-.... ·- ' -- .~~by~ ___ JI IL/:.. ate: 4/1-tJ,itr. nme: 1~~Nam<t Tanner""""'-,,..., R .. lnquished by: 08!0! --Time: ~Nerne; RelinqUfollod Cly: Date: ~~- ITlme: °""..,Name: ·-by: Date: b.nalLR trm1e: !'ml Name: Time Samoled 1345 --~- 1335 10SS --- 1420 1135 133S - ~ - ---- - Received by: l'"°!latln CHAIN OF CUSTODY All analysls wtn be cooducled using NBAP accredited methods and all dala wtll be reported using AWl'J.'s ·-analyle lls1s and n,porting limi1s (POL) lnBSS speclflcally n,quested otherwise on tl1is Chain of CUsltJ<ly and/or attached documenlalion. I ,: QCLewl: \ I Tum Around Time: Unless o1her arrangements have been m-. signed rep()l1s wtn be emailed by 5:00 pm on 3 Standard lhe day they are due. X Include EDD: LOCUS UPLOAD .P ' EXCBI. ii X Field Filtered For: 1::-. J>taaol,recJ.Metai. ~ ' . . E i o' • For Compliance With: ~ . D NELAP c ~ i D RCRA . D CWA : '. ( ; D SOWA -D ELAP/A2LA ,.. . r : ! ( ' D NLLAP c~ t ! /. i -D Non-Compliance : 1 D Other: i D' I t ~ f! )( . .. ~ 0 i C: 5 ' 'I" c 1,• s ., ~ ' l/) '~ ' C: ::; : ~ i Known Hazards 0 .. i ; ' . 0 i5. ' i GIi • ' & E ~ 1! ., i ' Samole Comments "' 7 w : X ~ 7 w : X ~ ; 7 w : X : 7 w l X " 7 w !c J X ~ ' vV'll7_ '\ho.._\ blfo~.c V'\...._ 7 w k : X II l 7 w J X l 7 J X l 7 w I( : X It : ; 7 w : X ~ : 7 w X : : 3 w l ~M IJ\0~111 ) Date:4 l t;; 2-2-Special Instructions: AWAL Lab Sample Set# Page 1 of 1 r=D.,, Laboratory Use Only lsamp1es Were; vLf5 ~-~ :Z Amblenl ~ 3 Tem1*11tl.re D,°\-c 4 Reeelved Brl>kenll.eaklng (Improperly Sealed) y N 5 Property Preserved y N Checked at bench y N 6 Received WltNn " Holding Tm,es y N lcoc Tape Waa: 1 Praoent on Outer Package y N NA 2 UrtJroken on Outer Package y N NA 3 Present on Sample y N NA 4 Unbroken on Semple y N NA i)~ Between Sample '--and COC Reconl? y N """' ~f\~ B r-r 1 \ ... A'(\ nm,. I 'n~ 't.JO Sample containers for metals were field filtered. See the Recefwoby: Date: Analytical Scope of Work for Reporting Limits and voe analyte <:lnnat,n list. Time: 5/13/22 Bottles for TDS are all plain pints. KOM """"Narne: Received by: Date: Include TDS Ratio, calculating from 22D1197. Slanatt.n> rnme: fA.\--S o..1.-Name: 1-· -_.,_..., ... ., -~ Received by: Date: l«lnnature TRACKING #: 1 Z 187 V4V 03 9493 3454 tnme: Print Nar1.1e: I Analyte QC Sample ID: BWE0581-BLKI Date Prepared: 05/10/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0581-DUP1 Date Prepared: 05/10/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0581-BSI Date Prepared: 05/10/2022 Total Dissolved Solids (TDS) CtF WO#: 22E1133 www.ChemtechFord.com QC Report for Work Order (WO) -22E1133 %Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Blank -SM 2540 C Batch: BWE0581 Date Analyzed: 05/10/2022 ND 10 1.00 Duplicate -SM 2540 C Batch: BWE0581 QC Source Sample: 22Ell33-0l Date Analyzed: 05/10/2022 0.9 10 2820 2800 20 1.00 LCS -SM 2540 C Batch: BWE058 l Date Analyzed: 05/10/2022 98 90 -110 392 400 20 1.00 TabF Laboratory Analytical Reports -Accelerated Monitoring Tab Fl Laboratory Analytical Reports -Accelerated Monitoring May2022 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH•FORD Serving the lntermountain West Since 1953 LllB0RAT0RlES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-11_05042022 Matrix: Water Date Sampled: 5/4/22 11 :40 111111·1.!anir Chloride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \lctal, Manganese, Dissolved 59.5 1.6 1270 2290 0.254 Project Name: May Ground Water 2022 www.ChemtechFord.com mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 1.0 0.10 20.0 20 0.0100 PO#: Receipt: 5/6/22 12:00@ 1.7 °C Date Reported: 7/12/2022 Project Name: May Ground Water 2022 Sampled By: Tanner Holliday EPA300.0 EPA353.2 EPA300.0 SM 2540C EPA200,8 CtF WO#: 22E0524 Preparation Date/Time 5/11/22 5/9/22 5/19/22 5/9/22 5/16/22 Amended Lab ID: 22E0524-01 Analysis Date/Time 5/11/22 5/9/22 5/19/22 5/9/22 5/16/22 Page 3 of 23 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA80R,1,TORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-25_05032022 Matrix: Water Date Sampled: 5/3/22 12:25 lnori.:ank Total Dissolved Solids (TDS) 2660 Project Name: May Ground Water 2022 www.ChemtechFord.com mg/L Certificate of Analysis Minimum Reporting Limit 20 PO#: Receipt: 5/6/22 12:00@ 1.7 °C Date Reported: 7/12/2022 Project Name: May Ground Water 2022 Sampled By: Tanner Holliday SM2540C CtF WO#: 22E0524 Preparation Date/Time 5/9/22 Amended Lab ID: 22E0524-02 Analysis Date/Time 5/9/22 Page 4 of 23 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATOIIIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-26_05042022 Matrix: Water Date Sampled: 5/4/22 12:45 lnori.:anil- Chloride Nitrate+ Nitrite, Total, as N Total Dissolved Solids (TDS) \ olatih· Ori.:anit· ( ·ompountl, Chloroform 63.2 1.1 2860 616 Project Name: May Ground Water 2022 www.ChemtechFord.com mg/L mg/L mg/L ug/L Certificate of Analysis Minimum Reporting Limit 10.0 0.10 20 50.0 PO#: Receipt: 5/6/22 12:00@ 1.7 °C Date Reported: 7/12/2022 Project Name: May Ground Water 2022 Sampled By: Tanner Holliday EPA300.0 EPA353.2 SM2540C EPA 8260D /5030A CtF WO#: 22E0524 Preparation Date/Time 5/11/22 5/9/22 5/10/22 5/13/22 Amended Lab ID: 22E0524-03 Analysis Date/Time 5/11/22 5/9/22 5/10/22 5/13/22 Page 5 of 23 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-30_05042022 Matrix: Water Date Sampled: 5/4/22 10:25 I nori:ani, Chloride Nitrate+ Nitrite, Total, as N Total Dissolved Solids (TDS) \kral, Selenium, Dissolved Uranium, Dissolved 195 15 1640 0.0694 0.0101 Project Name: May Ground Water 2022 www.ChemtechFord.com mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 10.0 0.50 20 0.0050 0.0003 PO#: Receipt: 5/6/22 12:00@ 1.7 °C Date Reported: 7/12/2022 Project Name: May Ground Water 2022 Sampled By: Tanner Holliday EPA300.0 EPA353.2 SM2540C EPA200.8 EPA200.8 CtF WO#: 22E0524 Preparation Date/Time 5/11/22 5/9/22 5/9/22 5/16/22 5/16/22 Amended Lab ID: 22E0524-04 Analysis Date/Time 5/11/22 5/9/22 5/9/22 5/16/22 5/16/22 Page 6 of 23 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH•FORD Serving the lntermountain West Since 1953 LABO~ATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-31_05032022 Matrix: Water Date Sampled: 5/3/22 14:55 lnorganil Chloride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \krnl, Uranium, Dissolved 381 13 1220 2660 0.0229 Project Name: May Ground Water 2022 www.ChemtechFord.com mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 10.0 0.50 20.0 20 0.0003 PO#: Receipt: 5/6/22 12:00@ 1.7 °C Date Reported: 7/12/2022 Project Name: May Ground Water 2022 Sampled By: Tanner Holliday EPA300.0 EPA353.2 EPA300.0 SM 2540C EPA200.8 CtF WO#: 22E0524 Preparation Date/Time 5/11/22 5/9/22 5/12/22 5/9/22 5/16/22 Amended Lab ID: 22E0524-05 Analysis Date/Time 5/12/22 5/9/22 5/12/22 5/9/22 5/16/22 Page 7 of 23 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 1.AIO.,UOIIIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-65_05042022 Matrix: Water Date Sampled: 5/4/22 10:25 lnOl"l!llllil' Chloride Nitrate+ Nitrite, Total, as N Total Dissolved Solids (TDS) \!Nab Selenium, Dissolved Uranium, Dissolved 202 15 1600 0.0690 0.0101 Project Name: May Ground Water 2022 www.ChemtechFord.com mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 5.0 0.50 20 0.0050 0.0003 PO#: Receipt: 5/6/22 12:00@ 1.7 ·c Date Reported: 7/12/2022 Project Name: May Ground Water 2022 Sampled By: Tanner Holliday EPA300.0 EPA353.2 SM2540C EPA200.8 EPA200.8 CtF WO#: 22E0524 Preparation Date/Time 5/12/22 5/9/22 5/9/22 5/16/22 5/16/22 Amended Lab ID: 22E0524-06 Analysis Date/Time 5/12/22 5/9/22 5/9/22 5/16/22 5/16/22 Page 8 of 23 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 LABOR,\TORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 5/4/22 12:45 \ olatih· Orea nil' ( ·11mp11111HI, Chloroform < 1.0 Project Name: May Ground Water 2022 www.ChemtechFord.com ug/L Certificate of Analysis Minimum Reporting Limit 1.0 PO#: Receipt: 5/6/22 12:00@ 1.7 °C Date Reported: 7/12/2022 Project Name: May Ground Water 2022 Sampled By: Tanner Holliday EPA 8260D 15030A CtF WO#: 22E0524 Preparation Date/Time 5/11/22 Amended Lab ID: 22E0524-07 Analysis Date/Time 5/11/22 Page 9 of 23 9632 South 500 West CHEMTECH-FORD LA80RATORIES Amended 7/12/2022 Work Order: 22E0524 Pro,ject: Ma~' Ground Water 2022 Energy Fuels Resources, Inc. Attn: Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Client Service Contact: 801.262.7299 The analyses presented on this report were performed in accordance with the National Environmental Laboratory Accreditation Program (NELAP) unless noted in the comments, flags, or case narrative. If the report is to be used for regulatory compliance, it should be presented in its entirety, and not be altered. Approved By: Melissa Connolly, Project Manager Sandy, Utah 84070 801 .262.7299 Main 866.792.0093 Fax Serving the lntermountain West since 1953 www.ChemtechFord.com CH EMTECH-FORO LAllORATOll:11:S Amended Report Narrative Report Changes: Sample 22E0524-05RE did not apply to this report and has been removed. Energy Fuels Resources, Inc. Project: May Ground Water 2022 Project Manager: Tanner Holliday Laboratory ID 22E0524-01 22E0524-02 22E0524-03 22E0524-04 22E0524-05 22E0524-06 22E0524-07 Sample Name MW-11 _ 05042022 MW-25 _ 05032022 MW-26_05042022 MW-30_05042022 MW-31_05032022 MW-65_05042022 Trip Blank Work Order Report Narrative Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions There are no corrective actions associated with this work order. Project Name: May Ground Water 2022 www.ChemtechFord.com CtF WO#: 22E0524 I CHEMTECH•FORD lA60f;tATOAIES Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Amended Certificate of Analysis Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations ND= Not detected at the corresponding Minimum Reporting Limit (MRL). PO#: Receipt: 5/6/22 12:00 @ 1. 7 ·c Date Reported: 7/12/2022 Project Name: May Ground Water 2022 I mg/L = one milligram per liter or I mg/kg = one milligram per kilogram = I part per million. I ug/L = one microgram per liter or I ug/kg = one microgram per kilogram= I part per billion. I ng/L = one nanogram per liter or I ng/kg = one nanogram per kilogram = I part per trill ion. Project Name: May Ground Water 2022 www.ChemtechFord.com CtF WO#: 22E0524 Page 10 of 23 American West Analytical Laboratories 463 W. 3600 S. Salt Lake City, lJT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 ~ Fax# (801) 263-8687 Email awal@awaHabs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 8. Hwy. 191 Blanding, UT 84511 Contact Tanner Holliday Phone#: (435) 678-2221 Cell#: Email: tlao(1Jday@;C11.erc:,:fueb..com; lnreuieli'ii)m,."'Vft,ela.com; Project Name: May Ground Water 2022 Project#: PO#: Sampler Name: Tanner Holliday 22-BDS-:Z..(i' Samole ID: Date Samoled \ IIW-11 05042022 5/4/2022 ~ IMW-25 05032022 S/3/2022 '3 IIW-26 05042022 5/4/2022 ,t IIW-30 05042022 5/4/2022 ff JIW-31_05032022 5/3/2022 t JIW-65 05042022 5/4/2022 ' Trip Blank S/4/2022 0 , t Rolinqulshod by. _4 JJ. ~~ / / 110: ~t--otvt• ~ ,.,..aA•-~,., I/ Tlmo'. •r1ntNamo: T.,,,_Moll<lav 11"" ~-by. Colo; ............ Time: DrfntNamo: Roli--by. b ....... _ Cale: Time: ""-tNama: Rellnquiahed by: Date: i<,~nature rnme: PrfntN.,..: I Time Samoled 1140 1225 1245 1025 1455 1025 1245 llecelvecl by: ~nab.Jre Drif\tN1mo. Racolvecl by: "'~~- OrintName: Received by: 1c~-- in--. Namtt: Received by: ~~~---: CHAIN OF CUSTODY All anatyoia will be conducted using NELAP aa:redltad ~ and an data will be n,portad ualng AWAL's standard analyte llats end ._,ting 1;m11a (POL) unleo8 apecff'ocally requeotad otherwise on lhia Chain of CuslDdy and/or alUM;hed documontallon, QC Level: I Tum Around Time: Unl88A other arrangementa have been made, aigned -wtn be emailed by 5:00 pm on 3 Standard Iha day lhey ""' due. Ix lndudeEDD: LOCtJ8 UPLOAD &XCEi. Ix Field Filtered For: DIAoJved Metals 00 ca' 0 00 ca' ca' c::i AWAL Lab Sample Set# Page 1 of l°"oDMo, Laboratory Use Only ls.....w,-L).~:? (9-hand -- 2 Amblont €) 0 0 c::i c::i 0 For Compliance With: 3 Tompemur• il 'C C'I 0 0 "' ...... 0 "' "' ~ D NELAP t--C'I ;.::: ;.::: 0 RCRA 0 -c::i Q t--0 0 c::i ,::; 0 0 0 CWA 4 Racolved Elrokan/Leaklng ~ 0 0 ~ I() 0 SOWA (l~Seolad) 0 ~ ~ "' • ~ : ~ 0 ELAPIA2LA y N • 1 • g I • C) 0 NLLAP ~ ~ C) i c::i ! 0 Non-compliance 5 Propo,ty "'9Nrved II c::i ] a 0 ~ ~ 0 "Cl .! O') J! D Other: y N O') • dl .. 0 Checl<ed at bench e !'2. :a .. G' u :a 0 .. G> X 0 0 "Cl 0 0 y N C E t') "Cl 0 't' "Cl "Cl "Cl 0 :a !i "' i 1 0 l/) • .t .t • l/) u 6 Racoived Within C ::ii l/) ~ ~ .t ~ Known Hazards 0 G> -i ::t. i i i t3 Holdlng Tlmee u Q. N I! I • & 0 E 0 u 5l g y N .. i5 iS i5 i5 i5 Samole Comments .. fl) 2: f,,o 4 w X X X X X Qc., I w X X (J C 1 Preoent on Outer Paclcage 5 w X X X y N NA 4 w X X X X X (.' C-2 u-.onOuterP~ '-y N NA 4 w X X X X X 1w 3 P..-onsample 4 X X X X X y N NA 4 Ullbrolton on Sample 3 w X Y. N NA -Sample lAbels and C0C Record? y N J ) 0 Att 1 ~J..oJ~?liJ. ) 0!5"7;-J z.:z __ Special Instructions: ]:')p ..V'\I~ 1=<. {' I .L LI.}'"\ r-~2 r VO Sample containers for metals were field filtered. See the Date: Analytical Scope of Work for Reporting Limits and VOC analyte Time: list. Dale: UPS GROUND Time: -Oate: TRACKING#: 1Z 187 Y4Y 03 9348 7144 -lllme: I Work Order# 2-2 SOS 2t, Delivery Method: ~S D USPS dEx D Ch h Launer Courier l:' ~ j ::. ;J l i Q E J l .!I --Chemtech Lot I .;: u ~ .e li J l a, .z Sample# Container Preservative E ; --·b), f\.\-::> Ol.\ -01., kl i \ 'Sl r.., Ah -02-Ah -0~ -1\-D k_\ I \,\ ~ fr\.--i 01.(~~ -01 VI:/ 1~') ...... ! ~ I M~ s l Volume . 1111/mLI ff. CHEMTECH FORD LABORATORIES Sample Receipt Receiving Temperature ) .l ·c ' -.. ' '• ' . ' ,. - Comments J rl CH. (,\ I ~11rl. ~\\"'Al\+ Q \ \~ ~,-\ ,, \ \ t.;\'+ i .• I c:., \ l <s?...v-..:t "' \' 'O.::_-t,,"t 0 \~c1.,+ I CHEMTECH-FORD t .. \6CP'/':l,TOP.1€S sample Condition (check if yes I ~todySeals 0 Containers Intact ~can be matched to bottles ~eived on Ice 4,ect Conta;ners(s) r:::f Svfflcent Sample Volume D Headspace Present (VOC) D ~p(!rature Blank ifRtuived within Holding Time Plastic Containers A-PiastiCUnpreserved 8-Miscellaneous Plastic C-Cyanide Qt (NaOHJ E· Co!iform/Ecoli/HPC F· Sulfide Qt (Zn Acetate) L-Mercury 1631 M-Metals p;nt (HN03) N-Nutrient Pint (H2S04J R· Radiological IHN03J s. Sludge Cups(Tubs O· Plastic Bag Glass Containers O· 625 (Na25203) G· Glass Unpreserved H-HAAS (NH4CI) I-508/515/525 (Na2503) K· 515.3 Herbicides Q. Oil & Grease (HCI) p. Phenols (H2S04) T-TOC/TOX (H3P04) U-531 (MCAii, Na25203) v . 524/THMs (Ascorbic Acid} W-8260VOC (1'1 HCI) X· Vial Unpreserved V-624/504 (Na2S203) Z-Miscellaneous Glass Analyte QC Sample ID: BWE0745-BLK1 Date Prepared: 05/16/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWE0745-BS1 Date Prepared: 05/16/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWE0745-MS1 Date Prepared: 05 /16/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWE0745-MS2 Date Prepared: 05/16/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWE0745-MS3 Date Prepared: 05/16/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved CtF WO#: 22E0524 www.ChemtechFord.com QC Report for Work Order (WO) -22E0524 %Rec RPD Limits RPD Max Result Source Cone SpkValue MRL DF Blank -EPA 200.8 Batch: BWE0745 Date Analyzed: 05/16/2022 ND 0.0100 1.00 ND 0.0050 1.00 ND 0.0003 1.00 LCS -EPA 200.8 Batch: BWE0745 Date Analyzed: 05/16/2022 100 85 -115 0.040 0.0400 0.0005 1.00 100 85-115 0.040 0.0400 0.0005 1.00 102 85-115 0.041 0.0400 0.0003 1.00 Matrix Spike -EPA 200.8 Batch: BWE0745 QC Source Sample: 22E0524-0 l Date Analyzed: 05/16/2022 104 70 -130 0.296 0.254 0.0400 0.0005 1.00 114 70-130 0.057 0.011 0.0400 0.0005 1.00 99.1 70 -130 0.042 0.002 0.0400 0.0003 1.00 Batch: BWE0745 QC Source Sample: 22E0524-04 Date Analyzed: 05/16/2022 94.5 70 -130 0.045 0.007 0.0400 0.0005 1.00 99.8 70-130 0.109 0.069 0.0400 0.0005 1.00 102 70 -130 0.051 0.010 0.0400 0.0003 1.00 Batch: BWE0745 QC Source Sample: 22E0524-05 Date Analyzed: 05/16/2022 94.0 70 -130 0.038 0.0009 0.0400 0.0005 1.00 97.8 70-130 0.146 0.106 0.0400 0.0005 1.00 98.1 70 -130 0.062 0.023 0.0400 0.0003 1.00 QC Report for Work Order (WO) -22E0524 Analyte % Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Blank -EPA 300.0 QC Sample ID: BWE0451-BLK1 Batch: BWE0451 Date Prepared: 05/10/2022 Date Analyzed: 05/10/2022 Chloride ND 1.0 1.00 QC Sample ID: BWE0511-BLK1 Batch: B WE0511 Date Prepared: 05/11/2022 Date Analyzed: 05/11/2022 Chloride ND 1.0 1.00 Sulfate ND 1.0 1.00 QC Sample ID: BWE0513-BLK1 Batch: BWE0513 Date Prepared: 05/11 /2022 Date Analyzed: 05/11/2022 Chloride ND 1.0 1.00 QC Sample ID: BWE0527-BLK1 Batch: BWE0527 Date Prepared: 05/12/2022 Date Analyzed: 05/12/2022 Chloride ND 1.0 1.00 Sulfate ND 1.0 1.00 QC Sample ID: BWE0580-BLK1 Batch: BWE0580 Date Prepared: 05/12/2022 Date Analyzed: 05/12/2022 Chloride ND 1.0 1.00 QC Sample ID: BWE0604-BLK1 Batch: BWE0604 Date Prepared: 05/12/2022 Date Analyzed: 05/12/2022 Chloride ND 1.0 1.00 Sulfate ND 1.0 1.00 QC Sample ID: BWE0886-BLK1 Batch: BWE0886 Date Prepared: 05/18/2022 Date Analyzed: 05/18/2022 Sulfate ND 1.0 1.00 LCS -EPA 300.0 QC Sample ID: BWE0451-BS1 Batch: BWE0451 Date Prepared: 05/I0/2022 Date Analyzed: 05/11/2022 Chloride 99.4 90 -110 49.7 50.0 1.0 1.00 QC Sample ID: BWE0511-BS1 Batch: BWE0511 Date Prepared: 05/11/2022 Date Analyzed: 05/11 /2022 Chloride 99.7 90 -110 49.8 50.0 1.0 1.00 Sulfate 98.8 90 -110 49.4 50.0 1.0 1.00 QC Sample ID: BWE0513-BS1 Batch: BWE0513 Date Prepared: 05/11 /2022 Date Analyzed: 05/11/2022 Chloride 98.9 90 -110 49.4 50.0 1.0 1.00 QC Sample ID: BWE0527-BS1 Batch: BWE0527 Date Prepared: 05/12/2022 Date Analyzed: 05/12/2022 Chloride 99.0 90 -110 49.5 50.0 1.0 1.00 Sulfate 98.0 90 -110 49.0 50.0 1.0 1.00 QC Sample ID: BWE0580-BS1 Batch: BWE0580 Date Prepared: 05/12/2022 Date Analyzed: 05/12/2022 Chloride 100 90 -110 50.1 50.0 1.0 1.00 QC Sample ID: BWE0604-BS1 Batch: BWE0604 Date Prepared: 05/12/2022 Date Analyzed: 05/12/2022 Chloride 100 90 -110 50.1 50.0 1.0 1.00 Sulfate 99.6 90 -110 49.8 50.0 1.0 1.00 CtF WO#: 22E0524 www.ChemtechFord.com QC Report for work Order (WO) -22E0524 Analyte % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL LCS -EPA 300.0 (cont.) QC Sample ID: BWE0886-BS1 Batch: BWE0886 Date Prepared: 05/18/2022 Date Analyzed: 05/18/2022 Sulfate 97.9 90 -110 48.9 50.0 1.0 Matrix Spike -EPA 300.0 QC Sample ID: BWE0451-MS1 Batch: BWE0451 QC Source Sample: XXXXXXX-XX Date Prepared: 05/10/2022 Date Analyzed: 05/10/2022 Chloride 98.3 80 -120 603 111 500 55.0 QC Sample ID: BWE0451-MS2 Batch: BWE045 l QC Source Sample: 22£0524-01 Date Prepared: 05/10/2022 Date Analyzed: 05/10/2022 Chloride 99.7 80 -120 199 ND 200 22.0 QC Sample ID: BWE0511-MS1 Batch: BWE0511 QC Source Sample: 22£0524-01 Date Prepared: 05/11/2022 Date Analyzed: 05/11/2022 Chloride 90.1 80 -120 69.6 59.5 11.1 1.1 Sulfate 80 -120 ND ND 11.1 1.1 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). QC Sample ID: BWE0511-MS2 Batch: BWE0511 QC Source Sample: XXXXXXX-XX Date Prepared: 05/11/2022 Date Analyzed: 05/11/2022 Chloride 96.7 80 -120 127 29.8 100 11.0 Sulfate 102 80 -120 145 42.4 100 11.0 QC Sample ID: BWE0513-MSI Batch: BWE0513 QC Source Sample: 22£0524-03 Date Prepared: 05/11/2022 Date Analyzed: 05/11/2022 Chloride 99.5 80 -120 163 63.2 100 11.0 QC Sample ID: BWE0513-MS2 Batch: BWE0513 QC Source Sample: 22£0524-04 Date Prepared: 05/11/2022 Date Analyzed: 05/11/2022 Chloride 97.2 80 -120 292 195 100 11.0 QC Sample ID: BWE0527-MS1 Batch: BWE0527 QC Source Sample: XXXXXXX-XX Date Prepared: 05/12/2022 Date Analyzed: 05/12/2022 Chloride 88.9 80 -120 231 221 11.1 1.1 Sulfate 98.9 80 -120 16.9 5.9 11.1 1.1 QC Sample ID: BWE0527-MS2 Batch: BWE0527 QC Source Sample: 22£0524-05 Date Prepared: 05/12/2022 Date Analyzed: 05/12/2022 Chloride 89.6 80 -120 471 381 100 11.0 Sulfate 75.8 80 -120 1280 1210 100 11.0 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWE0580-MS1 Date Prepared: 05/12/2022 Chloride Batch: BWE0580 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/12/2022 66.8 80 -120 30500 27200 5000 QM-010 -The MS recovery was outside acceptance limits but passed Duplicate Spike acceptance limits. The batch was accepted based on the acceptability of the MSD as the batch Spike. QC Sample ID: BWE0580-MS2 Batch: BWE0580 QC Source Sample: XXXXXXX-XX Date Prepared: 05/12/2022 Date Analyzed: 05/12/2022 Chloride 98.9 80 -120 29000 24000 5000 CtF WO#: 22E0524 www.ChemtechFord.com 550 550 OF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 QC Report for Work Order (WO) -22E0524 Analyte %Rec RPD Limits RPD Max Result Source Cone SpkValue MRL Matrix Spike -EPA 300.0 (cont.) QC Sample ID: BWE0604-MS1 Batch: BWE0604 QC Source Sample: 22E0524-05 Date Prepared: 05/13/2022 Date Analyzed: 05/13/2022 Chloride 93.2 80 -120 577 391 200 22.0 Sulfate 89.4 80 -120 1400 1220 200 22.0 QC Sample ID: BWE0604-MS2 Batch: BWE0604 QC Source Sample: XXXXXXX-XX Date Prepared: 05/13/2022 Date Analyzed: 05/13/2022 Chloride 94.5 80 -120 16.1 5.6 11.1 1.1 Sulfate 96.5 80 -120 58.2 47.5 11.1 1.1 QC Sample ID: BWE0886-MS 1 Batch: BWE0886 QC Source Sample: XXXXXXX-XX Date Prepared: 05/18/2022 Date Analyzed: 05/18/2022 Sulfate 103 80 -120 66.8 55.4 11.1 1.1 QC Sample ID: BWE0886-MS2 Batch: BWE0886 QC Source Sample: XXXXXXX-XX Date Prepared: 05/18/2022 Date Analyzed: 05/18/2022 Sulfate 105 80 -120 14.0 2.3 11.1 1.1 QC Sample ID: BWE0886-MS3 Batch: BWE0886 QC Source Sample: 22E0524-01 Date Prepared: 05/18/2022 Date Analyzed: 05/19/2022 Sulfate 42.9 80 -120 1350 1270 200 20.0 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Matrix Spike Dup -EPA 300.0 QC Sample ID: BWE0451-MSD1 Batch: BWE0451 QC Source Sample: XXXXXXX-XX Date Prepared: 05/10/2022 Date Analyzed: 05/10/2022 Chloride 98.7 0.315 80 -120 20 605 111 500 55.0 QC Sample ID: BWE0451-MSD2 Batch: BWE0451 QC Source Sample: 22E0524-0l Date Prepared: 05/10/2022 Date Analyzed: 05/10/2022 Chloride 100 0.444 80 -120 20 200 ND 200 22.0 QC Sample ID: BWE0511-MSD1 Batch: BWE05 l 1 QC Source Sample: 22E0524-01 Date Prepared: 05/11/2022 Date Analyzed: 05/11/2022 Chloride 91.9 0.288 80 -120 20 69.8 59.5 11.1 1.1 Sulfate 80 -120 20 ND ND 11.1 1.1 E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWE051 l-MSD2 Date Prepared: 05/11/2022 Chloride Sulfate QC Sample ID: BWE0513-MSD1 Date Prepared: 05/11/2022 Chloride QC Sample ID: BWE0513-MSD2 Date Prepared: 05/11/2022 Chloride QC Sample ID: BWE0527-MSD1 Date Prepared: 05/12/2022 CtF WO#: 22E0524 www.ChemtechFord.com Batch: BWE0511 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/11/2022 94.6 1.71 80 -120 20 124 29.8 100 11.0 97.2 3.62 80 -120 20 140 42.4 100 11.0 Batch: BWE0513 QC Source Sample: 22E0524-03 Date Analyzed: 05/11/2022 101 0.693 80 -120 20 164 63.2 100 11.0 Batch: BWE0513 QC Source Sample: 22E0524-04 Date Analyzed: 05/11/2022 97.0 0.0924 80 -120 20 292 195 100 11.0 Batch: BWE0527 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/12/2022 DF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 QC Report for work Order (WO) -22E0524 Analyte %Rec RPO Limits RPO Max Result Source Cone Spk Value MRL Matrix Spike Dup -EPA 300.0 (cont.) QC Sample ID: BWE0527-MSD1 Batch: BWE0527 QC Source Sample: XXXXXXX-XX Date Prepared: 05/12/2022 Date Analyzed: 05/12/2022 Chloride 86.9 0.0950 80 -120 20 231 221 11.1 1.1 Sulfate 99.4 0.329 80 -120 20 16.9 5.9 11.1 1.1 QC Sample ID: BWE0527-MSD2 Batch: BWE0527 QC Source Sample: 22E0524-05 Date Prepared: 05/12/2022 Date Analyzed: 05/12/2022 Chloride 92.6 0.647 80 -120 20 474 381 100 11.0 Sulfate 87.0 0.875 80 -120 20 1290 1210 100 11.0 QC Sample ID: BWE0580-MSD1 Batch: BWE0580 QC Source Sample: XXXXXXX-XX Date Prepared: 05/12/2022 Date Analyzed: 05/12/2022 Chloride 97.3 4.86 80 -120 20 32000 27200 5000 550 QC Sample ID: BWE0580-MSD2 Batch: BWE0580 QC Source Sample: XXXXXXX-XX Date Prepared: 05/12/2022 Date Analyzed: 05/12/2022 Chloride 97.2 0.288 80 -120 20 28900 24000 5000 550 QC Sample ID: BWE0604-MSD1 Batch: BWE0604 QC Source Sample: 22E0524-05 Date Prepared: 05/13/2022 Date Analyzed: 05/13/2022 Chloride 100 2.44 80 -120 20 591 391 200 22.0 Sulfate 92.5 0.454 80 -120 20 1400 1220 200 22.0 QC Sample ID: BWE0604-MSD2 Batch: BWE0604 QC Source Sample: XXXXXXX-XX Date Prepared: 05/13/2022 Date Analyzed: 05/13/2022 Chloride 107 8.37 80 -120 20 17.5 5.6 11.1 1.1 Sulfate 102 1.12 80 -120 20 58.8 47.5 11.1 1.1 QC Sample ID: BWE0886-MSD1 Batch: BWE0886 QC Source Sample: XXXXXXX-XX Date Prepared: 05/18/2022 Date Analyzed: 05/18/2022 Sulfate 96.4 1.09 80 -120 20 66.1 55.4 11.1 1.1 QC Sample ID: BWE0886-MSD2 Batch: BWE0886 QC Source Sample: XXXXXXX-XX Date Prepared: 05/18/2022 Date Analyzed: 05/18/2022 Sulfate 94.4 8.80 80 -120 20 12.8 2.3 11.1 1.1 QC Sample ID: BWE0886-MSD3 Batch: BWE0886 QC Source Sample: 22E0524-0I Date Prepared: 05/18/2022 Date Analyzed: 05/19/2022 Sulfate 40.9 0.309 80 -120 20 1350 1270 200 20.0 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. CtF WO#: 22E0524 www.ChemtechFord.com OF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 QC Report for Work Order (WO) -22E0524 Analyte % Rec RPO Limits RPO Max Result Source Cone SpkValue Blank -EPA 353.2 QC Sample ID: BWE0378-BLK1 Batch: BWE0378 Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Nitrate+ Nitrite, Total, as N ND LCS -EPA 353.2 QC Sample ID: BWE0378-BS1 Batch: BWE0378 Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Nitrate + Nitrite, Total, as N 101 80 -120 2.0 2.00 Matrix Spike -EPA 353.2 QC Sample ID: BWE0378-MS2 Batch: BWE0378 QC Source Sample: XXXXXXX-XX Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Nitrate + Nitrite , Total, as N 102 80 -120 1.3 0.28 1.00 QC Sample ID: BWE0378-MS3 Batch: BWE0378 QC Source Sample: 22E0524-0 I Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Nitrate+ Nitrite, Total, as N 91.4 80 -120 2.5 1.6 1.00 QC Sample ID: BWE0378-MS4 Batch: BWE0378 QC Source Sample: 22E0524-03 Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Nitrate+ Nitrite, Total, as N 105 80 -120 2.1 1.1 1.00 QC Sample ID: BWE0378-MS5 Batch: BWE0378 QC Source Sample: 22E0524-04 Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Nitrate+ Nitrite, Total, as N 88.2 80 -120 16 15 1.00 QC Sample ID: BWE0378-MS6 Batch: BWE0378 QC Source Sample: 22E0524-05 Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Nitrate + Nitrite, Total, as N 90.7 80 -120 14 13 1.00 Matrix Spike Dup -EPA 353.2 QC Sample ID: BWE0378-MSD2 Batch: BWE0378 QC Source Sample: XXXXXXX-XX Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Nitrate+ Nitrite, Total, as N 104 1.37 80 -120 20 1.3 0.28 1.00 QC Sample ID: BWE0378-MSD3 Batch: BWE0378 QC Source Sample: 22E0524-01 Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Nitrate+ Nitrite, Total, as N 99.7 3.21 80 -120 20 2.6 1.6 1.00 QC Sample ID: BWE0378-MSD4 Batch: BWE0378 QC Source Sample: 22E0524-03 Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Nitrate+ Nitrite, Total, as N 97.3 3.73 80 -120 20 2.1 1.1 1.00 QC Sample ID: BWE0378-MSD5 Batch: BWE0378 QC Source Sample: 22E0524-04 Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Nitrate + Nitrite, Total, as N 76.4 0.726 80 -120 20 16 15 1.00 QM-12 -The MSD recovery was outside acceptance limits, but passed duplicate spike acceptance criteria. The batch was accepted based on the acceptability of the MS. QC Sample ID: BWE0378-MSD6 Batch: BWE0378 QC Source Sample: 22E0524-05 Date Prepared: 05/09/2022 Date Analyzed: 05/09/2022 Nitrate+ Nitrite, Total, as N CtF WO#: 22E0524 www.ChemtechFord.com 88.6 0.149 80 -120 20 14 13 1.00 MRL OF 0.10 1.00 0.10 1.00 0.10 1.00 0.10 1.00 0.10 1.00 0.50 5.00 0.50 5.00 0.10 1.00 0.10 1.00 0.10 1.00 0.50 5.00 0.50 5.00 QC Report tor work orcier (WO) -::.!::.!1:U5::.!4 Analyte %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 8260D /5030A QC Sample ID: BWE0559-BLK1 Batch: BWE0559 Date Prepared: 05/11/2022 Date Analyzed: 05/11/2022 Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 QC Sample ID: BWE0630-BLK1 Batch: BWE0630 Date Prepared: 05/13/2022 Date Analyzed: 05/13/2022 Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 LCS -EPA 8260D /5030A QC Sample ID: BWE0559-BS 1 Batch: BWE0559 Date Prepared: 05/11/2022 Date Analyzed: 05/11 /2022 Acetone 91 .5 80 -120 91 .5 100 10.0 1.00 Benzene 104 80 -120 10.4 10.0 1.0 1.00 Carbon Tetrachloride 94.6 80 -120 9.46 10.0 1.0 1.00 Chloroform 108 80 -120 10.8 10.0 1.0 1.00 Chloromethane 109 80 -120 10.9 10.0 1.0 1.00 Methyl Ethyl Ketone 99.6 80 -120 99.6 100 10.0 1.00 Methylene Chloride 104 80 -120 10.4 10.0 1.0 1.00 Naphthalene 82.8 80 -120 8.28 10.0 1.0 1.00 Tetrahydrofuran 80 -120 ND 20.0 1.0 1.00 Toluene 103 80-120 10.3 10.0 1.0 1.00 Xylenes, total 98.7 80 -120 29.6 30.0 1.0 1.00 QC Sample ID: BWE0630-BS1 Batch: BWE0630 Date Prepared: 05/13/2022 Date Analyzed: 05/13/2022 Acetone 110 70 -130 110 100 10.0 1.00 Benzene 109 70 -130 10.9 10.0 1.0 1.00 Carbon Tetrachloride 104 70 -130 10.4 10.0 1.0 1.00 Chloroform 99.9 70 -130 9.99 10.0 1.0 1.00 Chloromethane 86.8 70 -130 8.68 10.0 1.0 1.00 Methyl Ethyl Ketone 137 70-130 137 100 10.0 1.00 HB -Recovery for this parameter exceeded the upper acceptance limit. Associated sample(s) were all non-detect and therefore accepted and reported for this parameter. Methylene Chloride 120 70 -130 12.0 10.0 1.0 1.00 CtF WO#: 22E0524 www.ChemtechFord.com QC Report for Work Order (WO) -22E0524 Analyte % Rec RPO limits RPO Max Result Source Cone Spk Value MRL OF LCS -EPA 8260D /5030A (cont.) QC Sample ID: BWE0630-BS1 Batch: BWE0630 Date Prepared: 05/13/2022 Date Analyzed: 05/13/2022 Naphthalene 115 70 -130 11.5 10.0 1.0 1.00 Tetrahydrofuran 70 -130 ND 20.0 1.0 1.00 Toluene 106 70 -130 10.6 10.0 1.0 1.00 Xylenes, total 108 70 -130 32.4 30.0 1.0 1.00 Matrix Spike -EPA 8260D /5030A QC Sample ID: BWE0559-MSI Batch: BWE0559 QC Source Sample: XXXXXXX-XX Date Prepared: 05/11/2022 Date Analyzed: 05/11/2022 Acetone 98.1 70 -130 1230 ND 1250 125 1.00 Benzene 106 70 -130 133 ND 125 12.5 1.00 Carbon Tetrachloride 128 70 -130 160 ND 125 12.5 1.00 Chloroform 105 70 -130 131 ND 125 12.5 1.00 Chloromethane 111 70 -130 138 ND 125 12.5 1.00 Methyl Ethyl Ketone 91 .8 70 -130 1150 ND 1250 125 1.00 Methylene Chloride 108 70 -130 135 ND 125 12.5 1.00 Naphthalene 90.6 70 -130 113 ND 125 12.5 1.00 Tetrahydrofuran 70 -130 ND ND 250 12.5 1.00 Toluene 105 70-130 131 ND 125 12.5 1.00 Xylenes, total 105 70 -130 393 ND 375 12.5 1.00 QC Sample ID: BWE0630-MSI Batch: BWE0630 QC Source Sample: 22E0524-03 Date Prepared: 05/13/2022 Date Analyzed: 05/13/2022 Acetone 92.7 70 -130 464 ND 500 50.0 1.00 Benzene 102 70 -130 51.1 ND 50.0 5.0 1.00 Carbon Tetrachloride 102 70 -130 51.0 ND 50.0 5.0 1.00 Chloroform 32.8 70 -130 632 616 50.0 5.0 1.00 MS-Low -Estimated low due to Matrix Spike recovery. Chloromethane 73.9 70 -130 37.0 ND 50.0 5.0 1.00 Methyl Ethyl Ketone 114 70 -130 568 ND 500 50.0 1.00 Methylene Chloride 111 70 -130 55.4 ND 50.0 5.0 1.00 Naphthalene 96.8 70 -130 48.4 ND 50.0 5.0 1.00 Tetrahydrofuran 70 -130 ND ND 100 5.0 1.00 Toluene 103 70 -130 51.6 ND 50.0 5.0 1.00 Xylenes, total 102 70 -130 153 ND 150 5.0 1.00 Matrix Spike Dup -EPA 8260D /5030A QC Sample ID: BWE0559-MSD1 Batch: BWE0559 QC Source Sample: XXXXXXX-XX Date Prepared: 05/11/2022 Date Analyzed: 05/11 /2022 Acetone 98.6 0.549 70 -130 20 1230 ND 1250 125 1.00 Benzene 105 1.13 70 -130 20 132 ND 125 12.5 1.00 Carbon Tetrachloride 107 18.1 70 -130 20 134 ND 125 12.5 1.00 Chloroform 109 3.74 70 -130 20 136 ND 125 12.5 1.00 Chloromethane 115 3.90 70 -130 20 144 ND 125 12.5 1.00 Methyl Ethyl Ketone 96.3 4.76 70 -130 20 1200 ND 1250 125 1.00 Methylene Chloride 106 1.77 70 -130 20 133 ND 125 12.5 1.00 Naphthalene 86.7 4.40 70 -130 20 108 ND 125 12.5 1.00 Tetrahydrofuran 70 -130 20 ND ND 250 12.5 1.00 Toluene 105 0.191 70 -130 20 131 ND 125 12.5 1.00 Xylenes, total 104 1.06 70 -130 20 389 ND 375 12.5 1.00 QC Sample ID: BWE0630-MSD1 Batch: BWE0630 QC Source Sample: 22E0524-03 Date Prepared: 05/13/2022 Date Analyzed: 05/13/2022 Acetone 91.4 1.49 70 -130 20 457 ND 500 50.0 1.00 CtF WO#: 22E0524 www.ChemtechFord.com QC Report tor work oraer (WO) -22EU524 Analyte %Rec RPD Limits RPD Max Result Source Cone Matrix Spike Dup -EPA 8260D /5030A (cont.) QC Sample ID: BWE0630-MSD1 Batch: BWE0630 QC Source Sample: 22£0524-03 Date Prepared: 05/13/2022 Date Analyzed: 05/13/2022 Benzene 103 0.974 70 -130 20 51 .6 ND Carbon Tetrachloride 99.5 2.38 70 -130 20 49.8 ND Chloroform -2.10 227 70 -130 20 614 616 MS-Low -Estimated low due to Matrix Spike recovery. Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total CtF WO#: 22E0524 www.ChemtechFord.com 77.1 4.24 111 2.26 111 0.181 93.5 3.47 100 2.55 104 2.07 70 -130 20 38.6 ND 70 -130 20 555 ND 70 -130 20 55.4 ND 70 -130 20 46.8 ND 70 -130 20 ND ND 70 -130 20 50.2 ND 70 -130 20 156 ND Spk Value MRL DF 50.0 5.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 500 50.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 100 5.0 1.00 50.0 5.0 1.00 150 5.0 1.00 Analyte QC Sample ID: BWE0372-BLK1 Date Prepared: 05/09/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0372-BS1 Date Prepared: 05/09/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0372-DUP1 Date Prepared: 05/09/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0372-DUP2 Date Prepared: 05 /09/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0386-BLK1 Date Prepared: 05/09/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0386-BSI Date Prepared: 05/09/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0386-DUPI Date Prepared: 05/09/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0386-DUP2 Date Prepared: 05/09/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0428-BLK1 Date Prepared: 05/10/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0428-DUP1 Date Prepared: 05/10/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0428-DUP2 Date Prepared: 05/10/2022 Total Dissolved Solids (TDS) QC Sample ID: BWE0428-BS1 Date Prepared: 05/10/2022 Total Dissolved Solids (TDS) CtF WO#: 22E0524 www.ChemtechFord.com QC Report for Work Order (WO) -22E0524 % Rec RPD Limits RPD Max Result Source Cone Batch: BWE0372 Date Analyzed: 05/09/2022 ND Batch: BWE0372 Date Analyzed: 05/09/2022 100 90 -110 400 Batch: BWE0372 QC Source Sample: 22E0524-05 Date Analyzed: 05/09/2022 4 10 2560 2660 Batch: BWE0372 QC Source Sample: 22E0524-0 I Date Analyzed: 05/09/2022 0.3 10 2300 2290 Batch: BWE0386 Date Analyzed: 05/09/2022 ND Batch: BWE0386 Date Analyzed: 05 /09/2022 100 90 -110 400 Batch: BWE0386 QC Source Sample: 22E0524-04 Date Analyzed: 05/09/2022 0.7 10 1630 1640 Batch: BWE0386 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/09/2022 2 10 2620 2580 Blank -SM 2540 C Batch: BWE0428 Date Analyzed: 05/10/2022 ND Duplicate -SM 2540 C Batch: BWE0428 QC Source Sample: 22E0524-03 Date Analyzed: 05/10/2022 0 10 2860 2860 Batch: BWE0428 QC Source Sample: XXXXXXX-XX Date Analyzed: 05/10/2022 10 10 54300 60300 LCS -SM 2540 C Batch: BWE0428 Date Analyzed: 05/10/2022 100 90 -110 400 Spk Value MRL DF 10 1.00 400 20 1.00 20 1.00 20 1.00 10 1.00 400 20 1.00 20 1.00 20 1.00 20 1.00 20 1.00 500 1.00 400 20 1.00 Surrogates Report for Work Order (WO) -22E0524 QC ID Analyte BWE0559-BLK1 1,2-Dichloroethane-d4 BWE0559-BLK1 4-Bromofluorobenzene BWE0559-BLK1 Toluene-dB BWE0630-BLK1 1,2-Dichloroethane-d4 BWE0630-BLK1 4-Bromofluorobenzene BWE0630-BLK1 Toluene-dB BWE0559-BS1 1,2-Dichloroethane-d4 BWE0559-BS1 4-Bromofluorobenzene BWE0559-BS1 Toluene-dB BWE0630-BS1 1,2-Dichloroethane-d4 BWE0630-BS1 4-Bromofluorobenzene BWE0630-BS1 Toluene-dB BWE0559-MS1 1,2-Dichloroethane-d4 BWE0559-MS1 4-Bromofluorobenzene BWE0559-MS1 Toluene-dB BWE0630-MS1 1,2-Dichloroethane-d4 BWE0630-MS1 4-Bromofluorobenzene BWE0630-MS1 Toluene-dB BWE0559-MSD1 1,2-Dichloroethane-d4 BWE0559-MSD1 4-Bromofluorobenzene BWE0559-MSD1 Toluene-dB BWE0630-MSD1 1,2-Dichloroethane-d4 BWE0630-MSD1 4-Bromofluorobenzene BWE0630-MSD1 Toluene-dB CtF WO#: 22E0524 www.ChemtechFord.com %Rec LCL UCL Result Blank -EPA 8260D /5030A 105 64.2 126 10.5 113 71.4 122 11 .3 99.8 63.2 129 9.98 90.6 64 .2 126 9.06 99.0 71.4 122 9.90 100 63.2 129 10.0 LCS -EPA 8260D /5030A 99.4 64.2 126 9.94 101 71.4 122 10.1 101 63.2 129 10.1 100 64.2 126 10.0 101 71.4 122 10.1 100 63.2 129 10.0 Matrix Spike -EPA 8260D /5030A 100 64.2 126 125 99.3 71.4 122 124 102 63.2 129 127 93.9 64.2 126 47.0 99.8 71 .4 122 49.9 100 63.2 129 50.0 Matrix Spike Dup -EPA 8260D /5030A 101 64.2 126 126 99.9 71 .4 122 125 101 63.2 129 126 90.7 64.2 126 45.4 99.9 71.4 122 50.0 97.1 63.2 129 48.6 SpkValue Batch DF 10.0 BWE0559 1.00 10.0 BWE0559 1.00 10.0 BWE0559 1.00 10.0 BWE0630 1.00 10.0 BWE0630 1.00 10.0 BWE0630 1.00 10.0 BWE0559 1.00 10.0 BWE0559 1.00 10.0 BWE0559 1.00 10.0 BWE0630 1.00 10.0 BWE0630 1.00 10.0 BWE0630 1.00 125 BWE0559 1.00 125 BWE0559 1.00 125 BWE0559 1.00 50.0 BWE0630 1.00 50.0 BWE0630 1.00 50.0 BWE0630 1.00 125 BWE0559 1.00 125 BWE0559 1.00 125 BWE0559 1.00 50.0 BWE0630 1.00 50.0 BWE0630 1.00 50.0 BWE0630 1.00 Surrogate Recoveries (Field Samples) LabNumber Analyte 8260 Low Level Volatiles 22E0524-03 Toluene-dB 22E0524-03 4-Bromofluorobenzene 22E0524-03 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22E0524-07 Toluene-dB 22E0524-07 22E0524-07 4-Bromofluorobenzene 1,2-Dichloroethane-d4 CtF WO#: 22E0524 www.ChemtechFord.com Result 10.0 9.81 9.23 9.88 10.5 9.83 Spklvl 10.0 10.0 10.0 10.0 10.0 10.0 %Rec 100 98.1 92.3 98 .8 105 98.3 LCL UCL Qualifier 63.2 129 71.4 122 64.2 126 63.2 129 71.4 122 64.2 126 TabF2 Laboratory Analytical Reports -Accelerated Monitoring June 2022 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 ll~BO!iit.\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-11_06062022 Matrix: Water Date Sampled: 6/6/22 12:20 l nor1.::mir Chloride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \kcal, Manganese, Dissolved 46.4 1.9 866 2360 0.228 Project Name: June Ground Water 2022 www.ChemtechFord.com mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 1.0 0.10 10.0 20 0.0100 PO#: Receipt: 6/9/22 15:00 @ 1.3 °C Date Reported: 6/22/2022 Project Name: June Ground Water 2022 Sampled By: Tanner Holliday EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 CtF WO#: 22F0888 Preparation Date/Time 6/15/22 6/20/22 6/15/22 6/10/22 6/15/22 Lab ID: 22F0888-01 Analysis Date/Time 6/15/22 6/20/22 6/15/22 6/10/22 6/15/22 Page 3 of20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA80RAfOIIIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-25_06072022 Matrix: Water Date Sampled: 6/7/22 10:35 l nor!!allil' Total Dissolved Solids (TDS) 2730 Project Name: June Ground Water 2022 www.ChemtechFord.com mg/L Certificate of Analysis Minimum Reporting !J..m.ti 20 PO#: Receipt: 6/9/22 15:00 @ 1.3 °C Date Reported: 6/22/2022 Project Name: June Ground Water 2022 Sampled By: Tanner Holliday SM2540C CtF WO#: 22F0888 Preparation Date/Time 6/10/22 Lab ID: 22F0888-02 Analysis Date/Time 6/10/22 Page 4 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATOR1ES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-26_06072022 Matrix: Water Date Sampled: 6/7/22 12:30 lnori.::mir Chloride Nitrate+ Nitrite, Total, as N Total Dissolved Solids (TDS) \ olatill· Oq!anir ( 11mpm111u, Acetone Benzene Carbon Tetrachloride Chloroform Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total 47.4 0.60 3120 <20.0 < 1.0 < 1.0 1250 < 1.0 <20.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Project Name: June Ground Water 2022 www.ChemtechFord.com mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis Minimum Reporting Limit 1.0 0.10 20 20.0 1.0 1.0 100 1.0 20.0 1.0 1.0 1.0 1.0 1.0 PO#: Receipt: 6/9/22 15:00 @ 1.3 °C Date Reported: 6/22/2022 Project Name: June Ground Water 2022 Sampled By: Tanner Holliday EPA300.0 EPA353.2 SM2540C EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22F0888 Preparation Date/Time 6/15/22 6/20/22 6/10/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 Lab ID: 22F0888-03 Analysis Date/Time 6/15/22 6/20/22 6/10/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 MS-High MS-Low Page 5 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/~B0fi1AT0RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-30_06072022 Matrix: Water Date Sampled: 6/7/22 10:25 l1111ri!anil" Chloride Nitrate+ Nitrite, Total, as N Total Dissolved Solids (IDS) \lctab Selenium, Dissolved Uranium, Dissolved 126 II 1660 0.0657 0.0096 Project Name: June Ground Water 2022 www.ChemtechFord.com mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 10.0 0.50 20 0.0050 0.0003 PO#: Receipt: 6/9/22 15:00 @ 1.3 °C Date Reported: 6/22/2022 Project Name: June Ground Water 2022 Sampled By: Tanner Holliday EPA300.0 EPA353.2 SM2540C EPA200.8 EPA200.8 CtF WO#: 22F0888 Preparation Date/Time 6/15/22 6/13/22 6/10/22 6/15/22 6/15/22 Lab ID: 22F0888-04 Analysis Date/Time 6/15/22 6/13/22 6/10/22 6/15/22 6/15/22 Page 6 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABO~!HO RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-31_06062022 Matrix: Water Date Sampled: 6/6/22 13:30 lnor1.:anif Chloride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (IDS) \ktal, Uranium, Dissolved 351 13 lllO 2690 0.0215 Project Name: June Ground Water 2022 www.ChemtechFord.com mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 10.0 0.50 20.0 20 0,0003 PO#: Receipt: 6/9/22 15:00 @ 1.3 °C Date Reported: 6/22/2022 Project Name: June Ground Water 2022 Sampled By: Tanner Holliday EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 CtF WO#: 22F0888 Preparation Date/Time 6/15/22 6/13/22 6/20/22 6/10/22 6/15/22 Lab ID: 22F0888-05 Analysis Date/Time 6/16/22 6/13/22 6/21/22 6/10/22 6/15/22 Page 7 of 20 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA60Fl:.loTORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-65_06072022 Matrix: Water Date Sampled: 6/7/22 10:35 lnuq::mir Total Dissolved Solids (TDS) 2540 Project Name: June Ground Water 2022 www.ChemtechFord.com mg/L Certificate of Analysis Minimum Reporting Limit 20 PO#: Receipt: 6/9/22 15:00 @ 1.3 °C Date Reported: 6/22/2022 Project Name: June Ground Water 2022 Sampled By: Tanner Holliday SM2540C CtF WO#: 22F0888 Preparation Date/Time 6/10/22 Lab ID: 22F0888-06 Analysis Date/Time 6/10/22 Page 8 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 6/7/22 12:30 \ olatill' Or:.?anil· ( ·ompounlb Acetone Benzene Carbon Tetrachloride Chloroform Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene X y lenes, total <20.0 < 1.0 < 1.0 < 1.0 < 1.0 <20.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Project Name: June Ground Water 2022 www.ChemtechFord.com ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis Minimum Reporting Limit 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 PO#: Receipt: 6/9/22 15:00 @ 1.3 °C Date Reported: 6/22/2022 Project Name: June Ground Water 2022 Sampled By: EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22F0888 Preparation Date/Time 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 Lab ID: 22F0888-07 Analysis Date/Time 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 6/17/22 Page 9 of 20 9632 South 500 West CHEMTECH·FORD LABORATORIES 6/22/2022 Work Order: 22 F0888 Pro,jcct: .June Ground Water 2022 Energy Fuels Resources, Inc. Attn: Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Client Service Contact: 801.262.7299 The analyses presented on this report were performed in accordance with the National Environmental Laboratory Accreditation Program (NELAP) unless noted in the comments, flags, or case narrative. If the report is to be used for regulatory compliance, it should be presented in its entirety, and not be altered. Approved By: Melissa Connolly, Project Manager Sandy, Utah 84070 801.262.7299 Main 866.792.0093 Fax Serving the lntermountain West since 1953 www.ChemtechFord.com CHEMTECH-FORD LABORATORl!::S Energy Fuels Resources, Inc. Project: June Ground Water 2022 Project Manager: Tanner Holliday Laboratory ID 22F0888-01 22F0888-02 22F0888-03 22F0888-04 22F0888-05 22F0888-06 22F0888-07 Sample Name MW-11_06062022 MW-25_06072022 MW-26_06072022 MW-30_ 06072022 MW-31 _06062022 MW-65_06072022 Trip Blank Work Order Report Narrative Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions There are no corrective actions associated with this work order. Project Name: June Ground Water 2022 www.ChemtechFord.com CtF WO#: 22F0888 CHEMTECH·FORD t.ABOIQt\TOIIIES Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Certificate of Analysis Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations ND~ Not detected at the corresponding Minimum Reporting Limit (MRL). PO#: Receipt: 6/9/22 15:00@ 1.3 °C Date Reported: 6/22/2022 Project Name: June Ground Water 2022 I mg/L ~ one milligram per liter or I mg/kg~ one milligram per kilogram ~ I part per mill ion. I ug/L ~ one microgram per liter or 1 ug/kg ~ one microgram per kilogram~ I part per billion. I ng/L ~ one nanogram per liter or I ng/kg ~ one nano gram per kilogram ~ 1 part per trillion. Flag Descriptions MS-High~ Estimated high due to Matrix Spike recovery. MS-Low~ Estimated low due to Matrix Spike recovery, Project Name: June Ground Water 2022 www.ChemtechFord.com CtF WO#: 22F0888 Page 10 of 20 3 ) I ! 3 American West Analytical Laboratories 463 W. 3600 S. Sall Lake City, UT 84115 Phone# (801) 263--8686 Toll Free# (888) 263-8686 L-~ Fax# (801) 263-8687 Email awal@awaHabs.com www.awal-labs.com Client: Enerey Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: Email: tlaollida:,(,tileaeq:,faela.eom; 11:weiDet@enerafaela.eom; Project Name: June Ground Water 2022 Project#: PO#: Sampler Name: Tanner Holliday Date Samele ID: Sameled IIW-11_06062022 6/6/2022 illW-25_06072022 6/7/2022 IIW-26_06072022 6/7/2022 IIW-30_06072022 6/7/2022 IIW-31_06062022 6/6/2022 IIW-65_06072022 6/7/2022 Trip Blank 6/7/2022 Relinqulohed by:_,, II II• / • ate: ""'""bJJ9 --...i -• -• -61812"'' Tanner HoJlklau .......J Time· Print Name: 11"" Relinquished by: Date: <:innalure llme: Print Name.: Relinqulohed by. Oato: s ....... -'Time• ~-, Relinquiohed by: Date: '<:1nnatun, rnme: PrintN-. I Time Sampled 1220 1035 1230 1025 1330 1035 1230 Received by: 51n ... - CHAIN OF CUSTODY All analyaia w111 be conducted ualng NELAP acaedlled melhodo and aN data will be reported using AWAL'• alandard analyto llolll and ,-.ting ttmlts (PQl) unleas apecifk:aJly requested olhe<wlae on this Chain of CU8tody and/or at1ached documen-. QC Level: I Tum Around Time: Unlesa other arrangement& have been made, algned reporto will be emailed by 5:00 pm on 3 Standard the day they are due. X Include EDD: LOCUS UPLOAD EXCEL X Field Filtered For: Diuolved lletala 00 a3' 0 00 a3' a3' ci 0 c:i ci ci 0 For Compliance With: N 0 0 "' i::' 0 "' "' ~ 0 NELAP N ~ ~ c:i --ci Cl D RCRA 0 t--0 0 0 0 CWA c:i 0 N 0 0 ~ I() 0 SOWA -0 ~ ~ "' u N u • -9 9 • ~ O ELAP/A2LA u 1 u o' 0 NLLAP ! Cl = 0 8 ~ ci i -a 1111 0 O Non-Compliance ~ 5 0 a "Cl .! = "' .g 0 Other: "' • ~ .. 0 e ~ :a .. G' ;:i 0 :a 0 .. CD " 0 0 0 0 C :s l'I "Cl "Cl "Cl "Cl "Cl 0 :a ]i .. 0 u 0 "' i u u u It) ::i; .t <:, It) .t .t .t u Known Hazards 8 II: It) ~ ::t. .. -I ::t. I I I • a N ! • 0 & 'o E i u i ~ .. c,l i5 f,,, i5 i5 i5 i5 Samele Comments 4 w X X X X X I w X 6 w X X X X 4 1W X X X X X 4 w X X X X X 1 w X X Data: Special Instructions: 'Tlmo: A :z, F""' O'i:;· b'~ ~, AWAL Lab Sample Set# Page or lo,e oa,e Laboratory Use Only Samples w.,., 1 Shipped or hand doltvllRld 2 Ambient or Chltled 3 Tempantuta lL·c ~ Roailv«l lkokonll.Nklng (lmproperty Sealed) y N 5 Properly p........,ed y N Ched<ed at bench y N 6 Received Within HoldingT,mes y N 1 P,-rt on Outw P"""- y N NA 2 Unbroken on Outer Padcage y N NA 3 Preoanl on Sample y N NA 4 Unbroken on Sample y N NA -Sample l.abola and COC Recon!7 y N "rtnlName, / Sample contamers for metals were field filtered. See the -~; c6!-, ,-/ "t'.i/~0 _, -Analytical Scope of Work for Reporting Limits and voe analyte --··-: .f t, '1 Print Nam...c. I: .., I-fr " I 'Tlme: list. "--/t.... 're.___ I /,~f! Raceivod by: I """'' --rr .... , PrlnlName: Raceived by. ~ ... , SlanalUre Time: Prln!Narna: I jl( I' 1111 .. Work Order# ,Z ·z Fl~>~;,-~- Delivery Method: ft UPS d ., ~ -. -. " ~'" ,, ~: ".[ Sample# () ( G 2-- G:'i (jt/ 0,) o Ct c::,7 D USPS Ch I·. "1~1 .... hC . Container r-/ ,C VIV VF7 l+l-"J N Li iJ /' .. 'N I<'/ L 1 / 1 \_,..j \...,,/T / :LJ ./.' I N l'Y) i:J L . ~~ ,.q,,, ./ V }J yY) ;::;/,-,. /~ '1_ ,.-,,_; i.}·) ouner Jurier I 111111111111 ~05615 :: a. E ] Chemtech Lot# :, ~ 0 or 1 Preservative -~~ /(fr;s !IS' 7 C /;'e_ f /V, k.~ "'I /1 t4[c.../ 11 err;; i("rf 1 C: //.__(- .::.li'-!~.f- i I ~-Ss/ ti,;, ? ~ /r'.:.. l· ' , f-Ci,., j, 1....._ -/1 / ,___ J ~r--(._/ j I i, <-;, I I ~7 -//...._ ::t I I '1, •.• ( ~ '-; ,· I ' I ;.1 ~-/ /,;.. L:,c..-I' I c. I -e..__;f-' ' ~ ~ g ~ :. .8 1! i ~ t .!! ~ u !i .!! j 0 .., "ii !i £ u: Misc .., i £ ~ .., Volume j j I!! l!l (oz/ml) _r;; CHEMTECH FORD LABORATORIES Sample Receipt Receiving Temperature /J ·c J t•--r -. -• I • . ' . ·., .!'-> ·jl -I 1. . ' .•, . . ~ ~ Comments • :r·.t'L ,. ... >· .._ CHEMTECH-FORD LAB0Rt,TQP.1E5 Sample Condition (check If yes) ~~ustody Seals Containers Intact COC can be matched to bottles Received on Ice Correct Containers(s) _Sufficent Sample Volume Received within Holding Time Plastic Containers A-Plastic Unpreserved B~ Miscellaneous Plastic C-Cyanide Qt (NaOH) E-Cohrorm/Ecoli/HPC F-Sulfide Qt {Zn Acetate) L-Mercury 1631 M-Metals Pint (HN03) N-Nutrient Pint (H2504) R-Radiological (HN03) S-Sludge Cups/Tubs 0-Plastic Bag Glass Containers D· 625 (Na2S203) G-Glass Unpreserved H· HAAs (NH4CI) J. 508/515/525 (Na2S03) K-5153 Herbicides 0-Oil & Grease (HCI) P· Phenols (H2S04) T-TOC/TOX (H3P04) U-531 (MCAA, Na252D3) V-524/rHMs (Ascorbic Acid) W-8260VOC (1:1 HCI) X-Vial Unpreserved Y· 624/S04 (Na25203) 2-Miscellaneous Glass Analyte QC Sample ID: BWF0734-BLK1 Date Prepared: 06/15/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWF0734-BSI Date Prepared: 06/15/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWF0734-MS1 Date Prepared: 06/15/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved CtF WO#: 22F0888 www.ChemtechFord.com QC Report for Work Order (WO) -22F0888 %Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -EPA 200.8 Batch: BWF0734 Date Analyzed: 06/15/2022 ND 0.0100 1.00 ND 0.0050 1.00 ND 0.0003 1.00 LCS -EPA 200.8 Batch: BWF0734 Date Analyzed: 06/15/2022 94.8 85 -115 0.038 0.0400 0.0005 1.00 94.9 85 -115 0.038 0.0400 0.0005 1.00 94.3 85 -115 0.038 0.0400 0.0003 1.00 Matrix Spike -EPA 200.8 Batch: BWF0734 QC Source Sample: 22F0888-0 I Date Analyzed: 06/15/2022 71.1 70 -130 0.256 0.228 0.0400 0.0005 1.00 109 70 -130 0.054 0.011 0.0400 0.0005 1.00 96.2 70 -130 0.041 0.002 0.0400 0.0003 1.00 Analyte QC Sample ID: BWF0762-BLKI Date Prepared: 06/15/2022 Chloride Sulfate QC Sample ID: BWFI012-BLKI Date Prepared: 06/20/2022 Sulfate QC Sample ID: BWF0762-BSI Date Prepared: 06/15/2022 Chloride Sulfate QC Sample ID: BWF1012-BSI Date Prepared: 06/20/2022 Sulfate QC Sample ID: BWF0762-MS I Date Prepared: 06/15/2022 Chloride QC Report for Work Order (WO) -22F0888 %Rec RPO Limits RPO Max Blank -EPA 300.0 Batch: BWF0762 Date Analyzed: 06/15/2022 Batch: BWFI012 Date Analyzed: 06/20/2022 LCS -EPA 300.0 Batch: BWF0762 Date Analyzed: 06/15/2022 97.6 90 -110 94.9 90 -110 Batch: BWF1012 Date Analyzed: 06/20/2022 Result ND ND ND 48.8 47.4 96.0 90 -110 48.0 Matrix Spike -EPA 300.0 Source Cone Batch: BWF0762 QC Source Sample: 22F0888-0l Date Analyzed: 06/16/2022 64.1 80 -120 53.6 46.4 Spk Value 50.0 50.0 50.0 11 .1 MRL 1.0 1.0 1.0 1.0 1.0 1.0 1.1 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. OF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 Sulfate -7790 80-120 ND 866 11.1 1.1 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is' considered an estimate (CLP E-flag). QC Sample ID: BWF0762-MS2 Batch: BWF0762 QC Source Sample: 22F0888-03 Date Prepared: 06/15/2022 Chloride Sulfate Date Analyzed: 06/16/2022 100 80 -120 -14100 80 -120 58.6 ND 47.4 1560 11.1 11.1 1.1 1.1 E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWF1012-MSI Batch: BWFI012 QC Source Sample: XXXXXXX-XX Date Prepared: 06/20/2022 Date Analyzed: 06/20/2022 Sulfate 88.2 80 -120 91.1 2.9 100 11 .0 QC Sample ID: BWF1012-MS2 Batch: BWF1012 QC Source Sample: XXXXXXX-XX Date Prepared: 06/20/2022 Date Analyzed: 06/20/2022 Sulfate 94.6 80 -120 112 17.6 100 11 .0 Matrix Spike Dup -EPA 300.0 QC Sample ID: BWF0762-MSD1 Batch: BWF0762 QC Source Sample: 22F0888-0l Date Prepared: 06/15/2022 Date Analyzed: 06/16/2022 Chloride 66.7 0.549 80 -120 20 53.8 46.4 11.1 1.1 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. CtF WO#: 22F0888 www.ChemtechFord.com 1.00 1.00 1.00 1.00 1.00 QC Report for Work Order (WO) -22F0888 Analyte % Rec RPD Limits RPD Max Result Source Cone Spk Value MRL QC Sample ID: BWF0762-MSD1 Date Prepared: 06/15/2022 Sulfate Matrix Spike Dup -EPA 300.0 (cont.) Batch: BWF0762 QC Source Sample: 22F0888-0l Date Analyzed: 06/16/2022 -7790 80 -120 20 ND 866 11.1 1.1 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). QC Sample ID: BWF0762-MSD2 Date Prepared: 06/15/2022 Chloride Sulfate Batch: BWF0762 QC Source Sample: 22F0888-03 Date Analyzed: 06/16/2022 96.6 0.719 80 -120 -14100 80 -120 20 20 58.2 ND 47.4 1560 11.1 11.1 1.1 1.1 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). QC Sample ID: BWF1012-MSD1 Batch: BWF1012 QC Source Sample: XXXXXXX-XX Date Prepared: 06/20/2022 Sulfate QC Sample ID: BWF1012-MSD2 Date Prepared: 06/20/2022 Sulfate CtF WO#: 22F0888 www.ChemtechFord.com Date Analyzed: 06/20/2022 89.8 1.75 80 -120 20 92.7 2.9 Batch: BWF1012 QC Source Sample: XXXXXXX-XX Date Analyzed: 06/20/2022 89.7 4.48 80 -120 20 107 17.6 100 11 .0 100 11 .0 DF 1.00 1.00 1.00 1.00 1.00 QC Report for Work Order (WO) -22F0888 Analyte % Rec RPD Limits RPD Max Result Source Cone SpkValue MRL DF Blank -EPA 353.2 QC Sample ID: BWF0598-BLK1 Batch: BWF0598 Date Prepared: 06/13/2022 Date Analyzed: 06/13/2022 Nitrate+ Nitrite, Total, as N ND 0.10 1.00 QC Sample ID: BWF0962-BLK1 Batch: BWF0962 Date Prepared: 06/20/2022 Date Analyzed: 06/20/2022 Nitrate + Nitrite, Total, as N ND 0.10 1.00 LCS -EPA 353.2 QC Sample ID: BWF0598-BS1 Batch: BWF0598 Date Prepared: 06/13/2022 Date Analyzed: 06/13/2022 Nitrate+ Nitrite, Total, as N 110 80 -120 2.2 2.00 0.10 1.00 QC Sample ID: BWF0962-BS1 Batch: BWF0962 Date Prepared: 06/20/2022 Date Analyzed: 06/20/2022 Nitrate + Nitrite, Total, as N 90.5 80 -120 1.8 2.00 0.10 1.00 Matrix Spike -EPA 353.2 QC Sample ID: BWF0598-MSI Batch: BWF0598 QC Source Sample: XXXXXXX-XX Date Prepared: 06/13/2022 Date Analyzed: 06/13/2022 Nitrate+ Nitrite, Total, as N 110 80 -120 1.3 0.17 1.00 0.10 1.00 QC Sample ID: BWF0598-MS2 Batch: BWF0598 QC Source Sample: XXXXXXX-XX Date Prepared: 06/13/2022 Date Analyzed: 06/13/2022 Nitrate + Nitrite, Total, as N 104 80 -120 1.3 0.22 1.00 0.10 1.00 QC Sample ID: BWF0962-MS1 Batch: BWF0962 QC Source Sample: 22F0888-01 Date Prepared: 06/20/2022 Date Analyzed: 06/20/2022 Nitrate+ Nitrite, Total, as N 79.2 80 -120 2.7 1.9 1.00 0.10 1.00 QM-010 -The MS recovery was outside acceptance limits but passed Duplicate Spike acceptance limits. The batch was accepted based on the acceptability of the MSD as the batch Spike. QC Sample ID: BWF0962-MS2 Batch: BWF0962 QC Source Sample: 22F0888-03 Date Prepared: 06/20/2022 Date Analyzed: 06/20/2022 Nitrate+ Nitrite, Total, as N 87.3 80 -120 1.5 0.60 1.00 0.10 1.00 QC Sample ID: BWF0962-MS3 Batch: BWF0962 QC Source Sample: XXXXXXX-XX Date Prepared: 06/20/2022 Date Analyzed: 06/20/2022 Nitrate+ Nitrite, Total, as N 100 80 -120 1.9 0.88 1.00 0.10 1.00 Matrix Spike Dup -EPA 353.2 QC Sample ID: BWF0598-MSD1 Batch: BWF0598 QC Source Sample: XXXXXXX-XX Date Prepared: 06/13/2022 Date Analyzed: 06/13/2022 Nitrate+ Nitrite, Total, as N 105 3.94 80 -120 20 1.2 0.17 1.00 0.10 1.00 QC Sample ID: BWF0598-MSD2 Batch: BWF0598 QC Source Sample: XXXXXXX-XX Date Prepared: 06/13/2022 Date Analyzed: 06/13/2022 Nitrate + Nitrite, Total, as N 106 1.73 80 -120 20 1.3 0.22 1.00 0.10 1.00 QC Sample ID: BWF0962-MSD1 Batch: BWF0962 QC Source Sample: 22F0888-01 Date Prepared: 06/20/2022 Date Analyzed: 06/20/2022 Nitrate+ Nitrite, Total, as N 95.1 5.79 80 -120 20 2.8 1.9 1.00 0.10 1.00 QC Sample ID: BWF0962-MSD2 Batch: BWF0962 QC Source Sample: 22F0888-03 Date Prepared: 06/20/2022 Date Analyzed: 06/20/2022 Nitrate+ Nitrite, Total, as N 91.9 3.07 80 -120 20 1.5 0.60 1.00 0.10 1.00 QC Sample ID: BWF0962-MSD3 Batch: BWF0962 QC Source Sample: XXXXXXX-XX Date Prepared: 06/20/2022 Date Analyzed: 06/20/2022 CtF WO#: 22F0888 www.ChemtechFord.com QC Report for Work Order (WO) -22F0888 Analyte %Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Blank -EPA 82600 /5030A QC Sample ID: BWF0873-BLK1 Batch: BWF0873 Date Prepared: 06/17/2022 Date Analyzed: 06/17/2022 Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 LCS -EPA 82600 /5030A QC Sample ID: BWF0873-BS1 Batch: BWF0873 Date Prepared: 06/1 6/2022 Date Analyzed: 06/16/2022 Acetone 93.5 70 -130 93.5 100 10.0 1.00 Benzene 106 70 -130 10.6 10.0 1.0 1.00 Carbon Tetrachloride 109 70-130 10.9 10.0 1.0 1.00 Chloroform 107 70 -130 10.7 10.0 1.0 1.00 Chloromethane 96.1 70 -130 9.61 10.0 1.0 1.00 Methyl Ethyl Ketone 104 70 -130 104 100 10.0 1.00 Methylene Chloride 108 70 -130 10.8 10.0 1.0 1.00 Naphthalene 118 70 -130 11.8 10.0 1.0 1.00 Tetrahydrofuran 84.9 70 -130 8.49 10.0 1.0 1.00 Toluene 109 70 -130 10.9 10.0 1.0 1.00 Xylenes, total 112 70 -130 33.5 30.0 1.0 1.00 Matrix Spike -EPA 82600 /5030A QC Sample ID: BWF0873-MS1 Batch: BWF0873 QC Source Sample: 22F0888-03 Date Prepared: 06/17/2022 Date Analyzed: 06/17/2022 Acetone 77.5 70 -130 1940 ND 2500 250 1.00 Benzene 81.4 70 -130 204 ND 250 25.0 1.00 Carbon Tetrachloride 76.7 70 -130 192 ND 250 25.0 1.00 Chloroform -255 70 -130 608 1250 250 25.0 1.00 MS-High -Estimated high due to Matrix Spike recovery. Chloromethane 62.1 70 -130 155 ND 250 25.0 1.00 MS-Low -Estimated low due to Matrix Spike recovery. Methyl Ethyl Ketone 87.6 70 -130 2190 ND 2500 250 1.00 Methylene Chloride 84.1 70 -130 210 ND 250 25.0 1.00 Naphthalene 94.8 70 -130 237 ND 250 25.0 1.00 Tetrahydrofuran 80.1 70 -130 200 ND 250 25.0 1.00 Toluene 83.0 70 -130 208 ND 250 25.0 1.00 Xylenes, total 83.4 70 -130 626 ND 750 25.0 1.00 Matrix Spike Oup -EPA 82600 /5030A QC Sample ID: BWF0873-MSD1 Batch: BWF0873 QC Source Sample: 22F0888-03 Date Prepared: 06/17/2022 Date Analyzed: 06/17/2022 Acetone 81 .7 5.20 70 -130 20 2040 ND 2500 250 1.00 Benzene 95.9 16.4 70 -130 20 240 ND 250 25.0 1.00 Carbon Tetrachloride 93.6 19.8 70 -130 20 234 ND 250 25.0 1.00 Chloroform -85.4 -99.7 70 -130 20 1030 1250 250 25.0 1.00 MS-High -Estimated high due to Matrix Spike recovery. CtF WO#: 22F0888 www.ChemtechFord.com Analyte QC Sample ID: BWF0873-MSD1 Date Prepared: 06/17/2022 Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total CtF WO#: 22F0888 www.ChemtechFord.com QC Report for Work Order (WO) -22F0888 %Rec RPO Limits RPO Max Result Source Cone Matrix Spike Dup -EPA 8260D /5030A (cont.) Batch: BWF0873 QC Source Sample: 22F0888-03 Date Analyzed: 06/17/2022 73.8 17.2 70 -130 20 184 ND 88.6 1.10 70 -130 20 2210 ND 96.9 14.1 70 -130 20 242 ND 105 10.5 70 -130 20 263 ND 77.5 3.30 70 -130 20 194 ND 98.2 16.8 70 -130 20 246 ND 101 19.1 70 -130 20 757 ND SpkValue MRL OF 250 25.0 1.00 2500 250 1.00 250 25.0 1.00 250 25.0 1.00 250 25.0 1.00 250 25.0 1.00 750 25.0 1.00 Analyte QC Sample ID: BWF0517-BLK1 Date Prepared: 06/10/2022 Total Dissolved Solids (TDS) QC Sample ID: BWF0517-DUP1 Date Prepared: 06/10/2022 Total Dissolved Solids (TDS) QC Sample ID: BWF05 l 7-DUP2 Date Prepared: 06/10/2022 Total Dissolved Solids (TDS) QC Sample ID: BWF0517-BS1 Date Prepared: 06/10/2022 Total Dissolved Solids (TDS) CtF WO#: 22F0888 www.ChemtechFord.com QC Report for Work Order (WO) -22F0888 % Rec RPD Limits RPD Max Result Source Cone Blank -SM 2540 C Batch: BWF05 l 7 Date Analyzed: 06/10/2022 ND Duplicate -SM 2540 C Batch: BWF0517 QC Source Sample: 22F0888-03 Date Analyzed: 06/10/2022 1 10 3160 3120 Batch: BWF05 l 7 QC Source Sample: 22F0888-0l Date Analyzed: 06/10/2022 3 10 2290 2360 LCS -SM 2540 C Batch: BWF05 l 7 Date Analyzed: 06/10/2022 102 90 -110 408 Spk Value MRL DF 10 1.00 20 1.00 20 1.00 400 20 1.00 Surrogates Report for Work Order (WO) -22F0888 QC ID Analyte % Rec LCL UCL Result SpkValue Blank -EPA 8260D /5030A BWF0873-BLK1 1,2-Dichloroethane-d4 88.1 64.2 126 8.81 10.0 BWF0873-BLK1 4-Bromofluorobenzene 89.1 71.4 122 8.91 10.0 BWF0873-BLK1 Toluene-dB 100 63.2 129 10.0 10.0 LCS -EPA 8260D /5030A BWF0873-BS1 1,2-Dichloroethane-d4 92.6 64.2 126 9.26 10.0 BWF0873-BS1 4-Bromofluorobenzene 90.6 71.4 122 9.06 10.0 BWF0873-BS1 Toluene-dB 100 63.2 129 10.0 10.0 Matrix Spike -EPA 8260D /5030A BWF0873-MS1 1,2-Dichloroethane-d4 87.9 64.2 126 220 250 BWF0873-MS1 4-Bromofluorobenzene 88.2 71.4 122 220 250 BWF0873-MS1 Toluene-dB 96.9 63.2 129 242 250 Matrix Spike Dup -EPA 8260D /5030A BWF0873-MSD1 1,2-Dichloroethane-d4 88.2 64.2 126 220 250 BWF0873-MSD1 4-Bromofluorobenzene 89.4 71.4 122 224 250 BWF0873-MSD1 Toluene-dB 100 63.2 129 250 250 Surrogate Recoveries (Field Samples) LabNumber Analyte Result Spklvl %Rec LCL UCL 8260 Low Level Volatiles 22F0888-03 Toluene-dB 22F0888-03 4-Bromofluorobenzene 22F0888-03 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22F0888-07 Toluene-dB 22F0888-07 22F0888-07 4-Bromofluorobenzene 1,2-Dichloroethane-d4 CtF WO#: 22F0888 www.ChemtechFord.com 9.58 8.94 8.93 10.0 8.74 8.16 10.0 10.0 10.0 10.0 10.0 10.0 95.8 89.4 89.3 100 87.4 81.6 63.2 129 71.4 122 64.2 126 63.2 129 71.4 122 64.2 126 Batch DF BWF0873 1.00 BWF0873 1.00 BWF0873 1.00 BWF0873 1.00 BWF0873 1.00 BWF0873 1.00 BWF0873 1.00 BWF0873 1.00 BWF0873 1.00 BWF0873 1.00 BWF0873 1.00 BWF0873 1.00 Qualifier TabG Quality Assurance and Data Validation Tables -1 G A Q uarter I Field QN QC Evaluation 1x Casing Location Volume Volume Pumped MW-01 19.48 39.06 MW-02 12.79 26.04 Mw.~osa :r.,e· 14.56:. MW-05 21.82 44.48 MW-11 29.25 58.59 MW-12 13.71 28.21 MW-14 17.69 36.89 MW-15 20.79 43.40 MW-17 26.03 58.59 MW-18 39.31 80.29 MW-19 54.10 108.50 MW-20, $.OS s;oo MW-22 31 .16 65.1 0 MW·.23 11,96·:: .2"4!96 MW·24', j,73 14.80'' MW.-2~A 7:s.4 1oits~ MW-25 22.13 45.57 MW-26 NA Continuously Pumped well MW-26 NA Continuously Pumped well MW-27 24.48 52.08 MW-27 24.01 49.91 MW-28 23.31 47.74 MW-29 18.38 41.23 MW-30 22.88 52.08 MW-31 39.78 80.29 MW-32 31.61 65.10 MW-32 31.40 65.10 MW-35 8.14 17.36 MW-36 7.26 15.19 MW'-37 .1Q(39 _l4,5 . -- -MW-38 . 2:T/' ,:~00 . - MW-39 24.95 52.08 MW-40 26.39 53.16 TW4-24 NA Continuously Pumped well MW-26 and TW4-24 are continually pumped wells. MW~oaa MW-20 MW 2~ MW-24A MW-38 were: 2x Casing Volume 38.96 25.58 14~;3.2 43.64 58.5 27.42 35.38 41.58 52.06 78.62 108.2 10.12 62.32 . 23JJ -f8,4S t~.6'6 44.26 48.96 48.02 46.62 36.76 45.76 79.56 63.22 62.8 16.28 14.52 . 20~78 554 49.9 52.78 Volume Check Conductivity RPD pH okay 1731 1730 0.06 7.20 7.19 okay 3677 3678 0.03 7.12 7.12 Pumoed_QW, .6802 ~1, &.i9 6.81 · ,. 6.83 , okay 2808 2797 0.39 7.29 7.29 okay 2978 2990 0.40 7.37 7.37 okay 4084 4079 0.12 6.62 6.62 okay 3838 3838 0.00 6.55 6.55 okay 4222 4225 0.07 6.81 6.82 okay 3656 3652 0.11 6.94 6.94 okay 3232 3230 0.06 6.57 6.57 okay 1349 1316 2.48 6.92 6.92 Pumoect orv 5485 S499 0:25 7.7.0 1, 7.~ okay 7557 7557 0.00 4.58 4.58 Pumt.ed Gry ffii 382~ 0,8$ 6i21 a.so f Ul'iiPed,Drv M21 . ·~ <h01 .ct-.ao: 4,tt1 . POmped f>l'Y ~Ol '4:4'1..0. G;,20 4.75 4i.7'9 okay 3145 3131 0.45 6.71 6.71 --3290 NC 6.70 -3333 NC 6.74 okay 1240 1240 0.00 7.37 7.37 okay 1192 1192 0.00 7.45 7.45 okay 4065 4071 0.15 6.24 6.24 okay 4548 4543 0.11 6.52 6.52 okay 2196 2202 0.27 6.92 6.92 okay 3355 3360 0.15 6.99 6.98 okay 3639 3642 0.08 6.52 6.51 okay 3727 3727 0.00 6.54 6.54 okay 4059 4070 0.27 6.71 6.71 okay 4820 4824 0.08 7.02 7.02 'Pum1:1ed .D1Y 4458 4467 o.~1 1.os 7:04 Piinir>ecl' Ofy· 42'l1 4262 0:21.-7,1W '1.13 okay 4693 4697 0.09 4.00 4.00 okay 3895 3901 0.15 6.77 6.76 -11117 NC 6.70 NM ::: Not Measured. The OAP does not require the measurement of redox potential or turbidity in wells that were purged to dryness. RPO = Relative Percent Difference RPD Temperature RPD Redox RPD Turbidity RPD 0.14 14.10 14.16 0.42 255 252 1.18 0 0 0.00 0.00 13.85 13.82 0.22 323 323 0.00 0 0 0.00 ·0:29~ 14.8.2 14.65 0:20, NM NC 11 · .. ' NM _ NC 0.00 15.66 15.40 1.67 307 303 1.31 0 0 0.00 0.00 14.57 14.53 0.27 334 333 0.30 45.0 46.0 2.20 0.00 14.78 14.75 0.20 322 322 0.00 0 0 0.00 0.00 14.95 14.94 0.07 319 319 0.00 0 0 0.00 0.15 14.95 14.96 0.07 324 325 0.31 0 0 0.00 0.00 15.01 15.05 0.27 329 330 0.30 4.6 4.7 2.15 0.00 16.40 16.30 0.61 322 322 0.00 0 0 0.00 0.00 15.20 15.10 0.66 312 313 0.32 0 0 0.00 0.78 16.40 16i32 Q.49 NM NC? NM NC 0.00 15.27 15.23 0.26 422 426 0.94 148.0 151.0 2.01 Q.48 14~11 14.10 0;!)7 NM -N©; ' NM .NQ Q~t .f 14'i4.1 14:';-35 -0;12 NM N!s.. -,fi_M. NG -~.a,; 16,40 15:2$ 011:_2 'NM Ne NM •f'ilG.:. 0.00 14.79 14.70 0.61 331 331 0.00 0 0 0.00 NC 16.70 NC 288 NC 1.0 NC N'.C 15.06 NC 336 NC 0 NC 0.00 14.58 14.60 0.14 305 304 0.33 0 0 0.00 0.00 15.28 15.26 0.13 349 349 0.00 1.0 1.0 0.00 0.00 15.60 15.65 0.32 336 336 0.00 1.1 1.2 8.70 0.00 14.21 14.19 0.14 267 266 0.38 9.3 9.3 0.00 0.00 15.13 15.87 4.77 300 301 0.33 0 0 0.00 0.14 14.98 14.92 0.40 269 269 0.00 0 0 0.00 0.15 14.85 14.82 0.20 283 281 0.71 98;0 99.0 1.02 0.00 15.31 15.31 0.00 265 264 0.38 43.2 43.3 0.23 0.00 14.40 14.42 0.14 306 305 0.33 0 0 0.00 0.00 14.35 14.30 0.35 278 278 0.00 0 0 0.00 0,57 ,• 1_:4.86 .1,4.80 ,, Q,40 ~M . R~, NM .N$, ,_ 0.1:.i, 1"5.68 15;60: ,0i5.f NM NG. I• NM .Ne 0.00 15.07 15.01 0.40 539 539 0.00 2.8 2.9 3.51 0.15 15.50 15.39 0.71 320 321 0.31 2.5 2.4 4.08 NC 16.56 NC 311 NC 4.1 NC The OAP states that turbidity should be less than 5 Nephelometric Turbidity Units ("NTUn) prior to sampling unless the well is characterized by water that has a higher turbidity. The OAP does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU are included for information purposes only. Dissolved Oxygen RPD 11.2 10.5 6.45 3.2 3.2 0.00 ,_-NM _ ·N~ 6.7 6.7 0.00 0 0 0.00 15.0 14.5 3.39 1.2 1.2 0.00 19.0 18.9 0.53 4.0 4.2 4.88 0 0 0.00 123.0 125.0 1.61 N.M Ne 10.7 10.5 1.89 1, NM NC ' NM NC ~ NM -~e 0 0 0.00 39.0 NC 23.4 NC 95.3 95.2 0.10 96.8 96.8 0.00 29.0 28.0 3.51 1.2 1.2 0.00 0 0 0.00 111.2 111.0 0.18 17.0 17.0 0.00 15.9 15.9 0.00 0 0 0.00 71.4 71 .6 0.28 . N~ " NG NM tilC 0 0 0.00 109.2 109.1 0.09 2010 NC G-1 B: Accelerated Field QA/QC Evaluation May 1x Casing 2x Casing Volume Dissolved Location Volume Volume Pumped Volume Check Conductivity RPD pH RPD Temperature RPD Redox RPD Turbidity RPD ox, gen RPD MW-11 29.31 59.67 58.62 okay 3083 I 3076 0.23 7.40 I 7.39 0.14 14.50 I 14.51 0.07 324 I 324 0.00 0 I 0 0.00 1.1 1 .1 0.00 MW-25 21.92 45.57 43.84 okay 3110 I 3115 0.16 6.84 I 6.84 0.00 15.09 I 15.04 0.33 324 I 324 0.00 75.0 I 75.0 0.00 4.9 4.8 2.06 MW-26 NA Continuously Pumped well --3548 NC 6.90 NC 15.80 NC 296 NC 0 NC 3_3.5 NC MW-30 22.78 45.57 45.56 okay 2197 I 2197 0.00 7.26 I 7.24 0.28 14.90 I 14.87 0.20 311 I 311 0.00 0 I 0 0.00 53.5 53.4 0.19 MW-31 39.70 80.29 79.4 okay 3328 I 3325 0.09 7.10 I 7.10 0.00 14.85 I 14.86 0.07 319 I 319 0.00 11.0 I 11.0 0.00 110.9 110.9 0.00 June 1x Casing 2x Casing Volume Dissolved Location Volume Volume Pumped Volume Check Conductivity RPD pH RPD Temperature RPD Redox RPD Turbidity RPD ox,rgen RPD MW-11 29.36 59.67 58.72 okay 3056 I 3067 0.36 7.50 I 7.50 0.00 15.38 I 15.40 0.13 433 I 427 1.40 132.0 I 134.o 1.50 2.9 2.9 0.00 MW-25 21.77 45.57 43.54 okay 3181 I 3176 0.16 6.90 I 6.88 0.29 15.69 I 15.60 0.58 475 I 477 0.42 1.0 I 1.0 0.00 52.0 51.0 1.94 MW026 NA Continuously Pumped well --3404 NC 6.84 NC 18.01 NC 277 NC 0 NC 29.0 NC MW-30 22.81 46.65 45.62 okay 2244 I 2230 0.63 7.35 I 7.32 0.41 15.20 I 15.15 0.33 476 I 478 0.42 0 I 0 0.00 52.6 52.5 0.19 MW-31 39.61 80.29 79.22 okay 3434 I 3424 0.29 7.16 I 7.13 0.42 15.45 I 15.48 0.19 465 I 465 0.00 1.1 I 1.0 9.52 114.0 114.0 0.00 -·-.. MW-261s a e0nt1nuall¥ pumped well. here are now Us-that were um · ed drY...m.:,;::::...:.:=.i:==~=---"'-----------------------------------------------------------------.............. ----- NM = Not Measured. The OAP does not require the measurement of redox potential or turbidity in wells that were purged to dryness. RPO = Relative Percent Difference The OAP states that turbidity should be less than 5 Nephelometric Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU are included for information purposes only. G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check Trip Blank Acetone 4/14/2022 4/26/2022 12 14 OK Trip Blank Benzene 4/14/2022 4/26/2022 12 14 OK Trip Blank Carbon Tetrachloride 4/14/2022 4/26/2022 12 14 OK Trip Blank Chloroform 4/14/2022 4/26/2022 12 14 OK Trip Blank Chloromethane 4/14/2022 4/26/2022 12 14 OK Trip Blank Methyl Ethyl Ketone 4/14/2022 4/26/2022 12 14 OK Trip Blank Methylene Chloride 4/14/2022 4/26/2022 12 14 OK Trip Blank Naphthalene 4/14/2022 4/26/2022 12 14 OK Trip Blank Tetrahydrofuran 4/14/2022 4/26/2022 12 14 OK Trip Blank Toluene 4/14/2022 4/26/2022 12 14 OK Trip Blank Xylenes, total 4/14/2022 4/26/2022 12 14 OK Trip Blank Acetone 4/18/2022 4/26/2022 8 14 OK Trip Blank Benzene 4/18/2022 4/26/2022 8 14 OK Trip Blank Carbon Tetrachloride 4/18/2022 4/26/2022 8 14 OK Trip Blank Chloroform 4/18/2022 4/26/2022 8 14 OK Trip Blank Chloromethane 4/18/2022 4/26/2022 8 14 OK Trip Blank Methyl Ethyl Ketone 4/18/2022 4/26/2022 8 14 OK Trip Blank Methylene Chloride 4/18/2022 4/26/2022 8 14 OK Trip Blank Naphthalene 4/18/2022 4/26/2022 8 14 OK Trip Blank Tetrahydrofuran 4/18/2022 4/26/2022 8 14 OK Trip Blank Toluene 4/18/2022 4/26/2022 8 14 OK Trip Blank Xylenes, total 4/18/2022 4/26/2022 8 14 OK Trip Blank Acetone 4/25/2022 5/3/2022 8 14 OK Trip Blank Benzene 4/25/2022 5/3/2022 8 14 OK Trip Blank Carbon Tetrachloride 4/25/2022 5/3/2022 8 14 OK Trip Blank Chloroform 4/25/2022 5/3/2022 8 14 OK Trip Blank Chloromethane 4/25/2022 5/3/2022 8 14 OK Trip Blank Methyl Ethyl Ketone 4/25/2022 5/3/2022 8 14 OK Trip Blank Methylene Chloride 4/25/2022 5/3/2022 8 14 OK Trip Blank Naphthalene 4/25/2022 5/3/2022 8 14 OK Trip Blank Tetrahvdrofuran 4/25/2022 5/3/2022 8 14 OK Trip Blank Toluene 4/25/2022 5/3/2022 8 14 OK Trip Blank Xylenes, total 4/25/2022 5/3/2022 8 14 OK Trip Blank Acetone 5/17/2022 5/25/2022 8 14 OK Trip Blank Benzene 5/17/2022 5/25/2022 8 14 OK Trip Blank Carbon Tetrachloride 5/17/2022 5/25/2022 8 14 OK Trip Blank Chloroform 5/17/2022 5/25/2022 8 14 OK Trip Blank Chloromethane 5/17/2022 5/25/2022 8 14 OK Trip Blank Methyl Ethyl Ketone 5/17/2022 5/25/2022 8 14 OK Trip Blank Methylene Chloride 5/17/2022 5/25/2022 8 14 OK Trip Blank Naphthalene 5/17/2022 5/25/2022 8 14 OK Trip Blank Tetrahyd.rofuran 5/17/2022 5/25/2022 8 14 OK Trip Blank Toluene 5/17/2022 5/25/2022 8 14 OK Trip Blank Xylenes, total 5/17/2022 5/25/2022 8 14 OK MW-01 Acetone 4/14/2022 4/26/2022 12 14 OK MW-01 Arsenic 4/14/2022 4/26/2022 12 180 OK MW-01 Benzene 4/14/2022 4/26/2022 12 14 OK MW-01 Beryllium 4/14/2022 4/26/2022 12 180 OK MW-01 Bicarbonate as CaC03 4/14/2022 4/16/2022 2 14 OK MW-01 Cadmium 4/14/2022 4/26/2022 12 180 OK MW-01 Calcium 4/14/2022 4/27/2022 13 180 OK MW-01 Carbon Tetrachloride 4/14/2022 4/26/2022 12 14 OK MW-01 Carbonate as C03 4/14/2022 4/16/2022 2 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-01 Chloride 4/14/2022 4/19/2022 5 28 OK MW-01 Chloroform 4/14/2022 4/26/2022 12 14 OK MW-01 Chloromethane 4/14/2022 4/26/2022 12 14 OK MW-01 Chromium 4/14/2022 4/26/2022 12 180 OK MW-01 Cobalt 4/14/2022 4/26/2022 12 180 OK MW-OJ Copper 4/14/2022 4/26/2022 12 180 OK MW-01 Fluoride 4/14/2022 5/4/2022 20 28 OK MW-01 Gross Radium Alpha 4/14/2022 5/10/2022 26 180 OK MW-01 Iron 4/14/2022 4/27/2022 13 180 OK MW-01 Lead 4/14/2022 4/26/2022 12 180 OK MW-01 Ma_gnesium 4/14/2022 4/27/2022 13 180 OK MW-01 Man_ganese 4/14/2022 4/26/2022 12 180 OK MW-OJ Mercury 4/14/2022 4/26/2022 12 180 OK MW-01 Methyl Ethyl Ketone 4/14/2022 4/26/2022 12 14 OK MW-01 Methylene Chloride 4/14/2022 4/26/2022 12 14 OK MW-01 Molybdenum 4/14/2022 4/26/2022 12 180 OK MW-01 Naphthalene 4/14/2022 4/26/2022 12 14 OK MW-01 Nickel 4/14/2022 4/26/2022 12 180 OK MW-01 Nitrate+ Nitrite as N 4/14/2022 4/21/2022 7 28 OK MW-01 Nitro_gen, Ammonia as N 4/14/2022 5/5/2022 21 28 OK MW-01 Potassium 4/14/2022 4/27/2022 13 180 OK MW-01 Selenium 4/14/2022 4/26/2022 12 180 OK MW-01 Silver 4/14/2022 4/26/2022 12 180 OK MW-01 Sodium 4/14/2022 4/27/2022 13 180 OK MW-01 Sulfate 4/14/2022 4/19/2022 5 28 OK MW-01 Tetrahydrofuran 4/14/2022 4/26/2022 12 14 OK MW-01 Thallium 4/14/2022 4/26/2022 12 180 OK MW-01 Tin 4/14/2022 4/27/2022 13 180 OK MW-01 Toluene 4/14/2022 4/26/2022 12 14 OK MW-01 Total Dissolved Solids 4/14/2022 4/19/2022 5 7 OK MW-01 Uranium 4/14/2022 4/26/2022 12 180 OK MW-01 Vanadium 4/14/2022 4/26/2022 12 180 OK MW-01 Xylenes, total 4/14/2022 4/26/2022 12 14 OK MW-01 Zinc 4/14/2022 4/26/2022 12 180 OK MW-02 Acetone 4/12/2022 4/25/2022 13 14 OK MW-02 Arsenic 4/12/2022 4/26/2022 14 180 OK MW-02 Benzene 4/12/2022 4/25/2022 13 14 OK MW-02 Beryllium 4/12/2022 4/26/2022 14 180 OK MW-02 Bicarbonate as CaC03 4/12/2022 4/16/2022 4 14 OK MW-02 Cadmium 4/12/2022 4/26/2022 14 180 OK MW-02 Calcium 4/12/2022 4/27/2022 15 180 OK MW-02 Carbon Tetrachloride 4/12/2022 4/25/2022 13 14 OK MW-02 Carbonate as C03 4/12/2022 4/16/2022 4 14 OK MW-02 Chloride 4/12/2022 4/19/2022 7 28 OK MW-02 Chloroform 4/12/2022 4/25/2022 13 14 OK MW-02 Chloromethane 4/12/2022 4/25/2022 13 14 OK MW-02 Chromium 4/12/2022 4/26/2022 14 180 OK MW-02 Cobalt 4/12/2022 4/26/2022 14 180 OK MW-02 Copper 4/12/2022 4/26/2022 14 180 OK MW-02 Fluoride 4/12/2022 5/4/2022 22 28 OK MW-02 Gross Radium Alpha 4/12/2022 5/10/2022 28 180 OK MW-02 Iron 4/12/2022 4/27/2022 15 180 OK MW-02 Lead 4/12/2022 4/26/2022 14 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-02 Magnesium 4/12/2022 4/27/2022 15 180 OK MW-02 Manganese 4/12/2022 4/26/2022 14 180 OK MW-02 Mercury 4/12/2022 4/26/2022 14 180 OK MW-02 Melhvl Ethyl Ketone 4/12/2022 4/25/2022 13 14 OK MW-02 Methylene Chloride 4/12/2022 4/25/2022 13 14 OK MW-02 Molybdenum 4/12/2022 4/26/2022 14 180 OK MW-02 Naphthalene 4/12/2022 4/25/2022 13 14 OK MW-02 Nickel 4/12/2022 4/26/2022 14 180 OK MW-02 Nitrate + Nitrite as N 4/12/2022 4/21/2022 9 28 OK MW-02 Nitrogen, Ammonia as N 4/12/2022 5/5/2022 23 28 OK MW-02 Potassium 4/12/2022 4/27/2022 15 180 OK MW-02 Selenium 4/12/2022 4/26/2022 14 180 OK MW-02 Silver 4/12/2022 4/26/2022 14 180 OK MW-02 Sodium 4/12/2022 4/27/2022 15 180 OK MW-02 Sulfate 4/12/2022 4/19/2022 7 28 OK MW-02 Tetrahydrofuran 4/12/2022 4/25/2022 13 14 OK MW-02 Thallium 4/12/2022 4/26/2022 14 180 OK MW-02 Tin 4/12/2022 4/27/2022 15 180 OK MW-02 Toluene 4/12/2022 4/25/2022 13 14 OK MW-02 Total Dissolved Solids 4/12/2022 4/18/2022 6 7 OK MW-02 Uranium 4/12/2022 4/26/2022 14 180 OK MW-02 Vanadium 4/12/2022 4/26/2022 14 180 OK MW-02 Xylenes, total 4/12/2022 4/25/2022 13 14 OK MW-02 Zinc 4/12/2022 4/26/2022 14 180 OK MW-03a Acetone 4/27/2022 5/3/2022 6 14 OK MW-03a Arsenic 4/27/2022 5/10/2022 13 180 OK MW-03a Benzene 4/27/2022 5/3/2022 6 14 OK MW-03a Beryllium 4/27/2022 5/10/2022 13 180 OK MW-03a Bicarbonate as CaC03 4/27/2022 5/3/2022 6 14 OK MW-03a Cadmium 4/27/2022 5/10/2022 13 180 OK MW-03a Calcium 4/27/2022 5/10/2022 13 180 OK MW-03a Carbon Tetrachloride 4/27/2022 5/3/2022 6 14 OK MW-03a Carbonate as C03 4/27/2022 5/3/2022 6 14 OK MW-03a Chloride 4/27/2022 5/8/2022 11 28 OK MW-03a Chloroform 4/27/2022 5/3/2022 6 14 OK MW-03a Chloromethane 4/27/2022 5/3/2022 6 14 OK MW-03a Chromium 4/27/2022 5/10/2022 13 180 OK MW-03a Cobalt 4/27/2022 5/10/2022 13 180 OK MW-03a Coooer 4/27/2022 5/10/2022 13 180 OK MW-03a Fluoride 4/27/2022 5/4/2022 7 28 OK MW-03a Gross Radium Alpha 4/27/2022 5/24/2022 27 180 OK MW-03a Iron 4/27/2022 5/11/2022 14 180 OK MW-03a Lead 4/27/2022 5/10/2022 13 180 OK MW-03a Magnesium 4/27/2022 5/10/2022 13 180 OK MW-03a Manganese 4/27/2022 5/10/2022 13 180 OK MW-03a Mercury 4/27/2022 5/4/2022 7 180 OK MW-03a Methyl E1hyl Ketone 4/27/2022 5/3/2022 6 14 OK MW-03a Methylene Chloride 4/27/2022 5/3/2022 6 14 OK MW-03a Molybdenum 4/27/2022 5/10/2022 13 180 OK MW-03a Naphthalene 4/27/2022 5/3/2022 6 14 OK MW-03a Nickel 4/27/2022 5/10/2022 13 180 OK MW-03a Nitrate+ Nitrite as N 4/27/2022 4/30/2022 3 28 OK MW-03a Nitrogen, Ammonia as N 4/27/2022 5/12/2022 15 28 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-03a Potassium 4/27/2022 5/10/2022 13 180 OK MW-03a Selenium 4/27/2022 5/10/2022 13 180 OK MW-03a Silver 4/27/2022 5/10/2022 13 180 OK MW-03a Sodium 4/27/2022 5/11/2022 14 180 OK MW-03a Sulfate 4/27/2022 5/24/2022 27 28 OK MW-03a Tetrahydrofuran 4/27/2022 5/3/2022 6 14 OK MW-03a Thallium 4/27/2022 5/10/2022 13 180 OK MW-03a Tin 4/27/2022 5/10/2022 13 180 OK MW-03a Toluene 4/27/2022 5/3/2022 6 14 OK MW-03a Total Dissolved Solids 4/27/2022 5/2/2022 5 7 OK MW-03a Uranium 4/27/2022 5/10/2022 13 180 OK MW-03a Vanadium 4/27/2022 5/10/2022 13 180 OK MW-03a Xylenes, total 4/27/2022 5/3/2022 6 14 OK MW-03a Zinc 4/27/2022 5/10/2022 13 180 OK MW-05 Acetone 4/18/2022 4/27/2022 9 14 OK MW-05 Arsenic 4/18/2022 5/2/2022 14 180 OK MW-05 Benzene 4/18/2022 4/27/2022 9 14 OK MW-05 Beryllium 4/18/2022 5/2/2022 14 180 OK MW-05 Bicarbonate as CaC03 4/18/2022 4/23/2022 5 14 OK MW-05 Cadmium 4/18/2022 5/2/2022 14 180 OK MW-05 Calcium 4/18/2022 5/2/2022 14 180 OK MW-05 Carbon Tetrachloride 4/18/2022 4/27/2022 9 14 OK MW-05 Carbonate as C03 4/18/2022 4/23/2022 5 14 OK MW-05 Chloride 4/18/2022 4/27/2022 9 28 OK MW-05 Chloroform 4/18/2022 4/27/2022 9 14 OK MW-05 Chloromethane 4/18/2022 4/27/2022 9 14 OK MW-05 Chromium 4/18/2022 5/2/2022 14 180 OK MW-05 Cobalt 4/18/2022 5/2/2022 14 180 OK MW-05 Copper 4/18/2022 5/2/2022 14 180 OK MW-05 Fluoride 4/18/2022 4/27/2022 9 28 OK MW-05 Gross Radium Alpha 4/18/2022 5/18/2022 30 180 OK MW-05 Iron 4/18/2022 5/2/2022 14 180 OK MW-05 Lead 4/18/2022 5/2/2022 14 180 OK MW-05 Magnesium 4/18/2022 5/2/2022 14 180 OK MW-05 Manganese 4/18/2022 5/2/2022 14 180 OK MW-05 Mercury 4/18/2022 5/3/2022 15 180 OK MW-05 Methyl Ethyl Ketone 4/18/2022 4/27/2022 9 14 OK MW-05 MetJ1ylene Chloride 4/18/2022 4/27/2022 9 14 OK MW-05 Molybdenum 4/18/2022 5/2/2022 14 180 OK MW-05 Naphthalene 4/18/2022 4/27/2022 9 14 OK MW-05 Nickel 4/18/2022 5/2/2022 14 180 OK MW-05 Nitrate + Nitrite as N 4/18/2022 4/25/2022 7 28 OK MW-05 Nitrogen, Ammonia as N 4/18/2022 5/5/2022 17 28 OK MW-05 Potassium 4/18/2022 5/2/2022 14 180 OK MW-05 Selenium 4/18/2022 5/2/2022 14 180 OK MW-05 Silver 4/18/2022 5/2/2022 14 180 OK MW-05 Sodium 4/18/2022 5/2/2022 14 180 OK MW-05 Sulfate 4/18/2022 4/27/2022 9 28 OK MW-05 Tetrahydrofuran 4/18/2022 4/27/2022 9 14 OK MW-05 Thallium 4/18/2022 5/2/2022 14 180 OK MW-05 Tin 4/18/2022 5/2/2022 14 180 OK MW-05 Toluene 4/18/2022 4/27/2022 9 14 OK MW-05 Total Dissolved Solids 4/18/2022 4/25/2022 7 7 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-05 Uranium 4/18/2022 5/2/2022 14 180 OK MW-05 Vanadium 4/18/2022 5/2/2022 14 180 OK MW-05 Xylenes, total 4/18/2022 4/27/2022 9 14 OK MW-05 Zinc 4/18/2022 5/2/2022 14 180 OK MW-11 Acetone 4/18/2022 4/27/2022 9 14 OK MW-11 Arsenic 4/18/2022 5/2/2022 14 180 OK MW-11 Benzene 4/18/2022 4/27/2022 9 14 OK MW-11 Beryllium 4/18/2022 5/2/2022 14 180 OK MW-11 Bicarbonate as CaC03 4/18/2022 4/23/2022 5 14 OK MW-11 Cadmium 4/18/2022 5/2/2022 14 180 OK MW-11 Calcium 4/18/2022 5/2/2022 14 180 OK MW-11 Carbon Tetrachloride 4/18/2022 4/27/2022 9 14 OK MW-11 Carbonate as C03 4/18/2022 4/23/2022 5 14 OK MW-11 Chloride 4/18/2022 4/27/2022 9 28 OK MW-11 Chloroform 4/18/2022 4/27/2022 9 14 OK MW-11 Chloromethane 4/18/2022 4/27/2022 9 14 OK MW-11 Chromium 4/18/2022 5/2/2022 14 180 OK MW-11 Cobalt 4/18/2022 5/2/2022 14 180 OK MW-11 Copper 4/18/2022 5/2/2022 14 180 OK MW-11 Fluoride 4/18/2022 5/2/2022 14 28 OK MW-11 Gross Radium Alpha 4/18/2022 5/18/2022 30 180 OK MW-11 Iron 4/18/2022 5/2/2022 14 180 OK MW-11 Lead 4/18/2022 5/2/2022 14 180 OK MW-11 Magnesium 4/18/2022 5/2/2022 14 180 OK MW-11 Manganese 4/18/2022 5/2/2022 14 180 OK MW-11 Mercury 4/18/2022 5/3/2022 15 180 OK MW-11 Methyl Ethyl Ketone 4/18/2022 4/27/2022 9 14 OK MW-11 Methylene Chloride 4/18/2022 4/27/2022 9 14 OK MW-11 Molybdenum 4/18/2022 5/2/2022 14 180 OK MW-11 Naphthalene 4/18/2022 4/27/2022 9 14 OK MW-11 Nickel 4/18/2022 5/2/2022 14 180 OK MW-11 Nitrate+ Nitrite as N 4/18/2022 4/25/2022 7 28 OK MW-11 Nitrogen, Ammonia as N 4/18/2022 5/5/2022 17 28 OK MW-11 Potassium 4/18/2022 5/2/2022 14 180 OK MW-11 Selenium 4/18/2022 5/2/2022 14 180 OK MW-11 Silver 4/18/2022 5/2/2022 14 180 OK MW-11 Sodium 4/18/2022 5/2/2022 14 180 OK MW-11 Sulfate 4/18/2022 4/27/2022 9 28 OK MW-11 Tetrahydrofuran 4/18/2022 4/27/2022 9 14 OK MW-11 Thallium 4/18/2022 5/2/2022 14 180 OK MW-11 Tin 4/18/2022 5/2/2022 14 180 OK MW-11 Toluene 4/18/2022 4/27/2022 9 14 OK MW-11 Total Dissolved Solids 4/18/2022 4/25/2022 7 7 OK MW-11 Uranium 4/18/2022 5/2/2022 14 180 OK MW-11 Vanadium 4/18/2022 5/2/2022 14 180 OK MW-11 Xylenes, total 4/18/2022 4/27/2022 9 14 OK MW-11 Zinc 4/18/2022 5/2/2022 14 180 OK MW-12 Acetone 4/19/2022 4/27/2022 8 14 OK MW-12 Arsenic 4/19/2022 5/2/2022 13 180 OK MW-12 Benzene 4/19/2022 4/27/2022 8 14 OK MW-12 Beryllium 4/19/2022 5/2/2022 13 180 OK MW-12 Bicarbonate as CaC03 4/19/2022 4/23/2022 4 14 OK MW-12 Cadmium 4/19/2022 5/2/2022 13 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-12 Calcium 4/19/2022 5/2/2022 13 180 OK MW-12 Carbon Tetrachloride 4/19/2022 4/27/2022 8 14 OK MW-12 Carbonate as C03 4/19/2022 4/23/2022 4 14 OK MW-12 Chloride 4/19/2022 4/27/2022 8 28 OK MW-12 Chloroform 4/19/2022 4/27/2022 8 14 OK MW-12 Chloromethane 4/19/2022 4/27/2022 8 14 OK MW-12 Chromium 4/19/2022 5/2/2022 13 180 OK MW-12 Cobalt 4/19/2022 5/2/2022 13 180 OK MW-12 Coooer 4/19/2022 5/2/2022 13 180 OK MW-12 Fluoride 4/19/2022 5/2/2022 13 28 OK MW-12 Gross Radium Alpha 4/19/2022 5/18/2022 29 180 OK MW-12 Iron 4/19/2022 5/2/2022 13 180 OK MW-12 Lead 4/19/2022 5/2/2022 13 180 OK MW-12 Magnesium 4/19/2022 5/2/2022 13 180 OK MW-12 Manganese 4/19/2022 5/2/2022 13 180 OK MW-12 Mercury 4/19/2022 5/3/2022 14 180 OK MW-12 Methyl Ethyl Ketone 4/19/2022 4/27/2022 8 14 OK MW-12 Methylene Chloride 4/19/2022 4/27/2022 8 14 OK MW-12 Molybdenum 4/19/2022 5/2/2022 13 180 OK MW-12 Naphthalene 4/19/2022 4/27/2022 8 14 OK MW-12 Nickel 4/19/2022 5/2/2022 13 180 OK MW-12 Nitrate + Nitrite as N 4/19/2022 4/25/2022 6 28 OK MW-12 Nitrogen, Ammonia as N 4/19/2022 5/5/2022 16 28 OK MW-12 Potassium 4/19/2022 5/2/2022 13 180 OK MW-12 Selenium 4/19/2022 5/2/2022 13 180 OK MW-12 Silver 4/19/2022 5/2/2022 13 180 OK MW-12 Sodium 4/19/2022 5/2/2022 13 180 OK MW-12 Sulfate 4/19/2022 4/27/2022 8 28 OK MW-12 Tetrahydrofuran 4/19/2022 4/27/2022 8 14 OK MW-12 Thallium 4/19/2022 5/2/2022 13 180 OK MW-12 Tin 4/19/2022 5/2/2022 13 180 OK MW-12 Toluene 4/19/2022 4/27/2022 8 14 OK MW-12 Total Dissolved Solids 4/19/2022 4/25/2022 6 7 OK MW-12 Uranium 4/19/2022 5/2/2022 13 180 OK MW-12 Vanadium 4/19/2022 5/2/2022 13 180 OK MW-12 Xylenes, total 4/19/2022 4/27/2022 8 14 OK MW-12 Zinc 4/19/2022 5/2/2022 13 180 OK MW-14 Acetone 4/18/2022 4/27/2022 9 14 OK MW-14 Arsenic 4/18/2022 5/2/2022 14 180 OK MW-14 Benzene 4/18/2022 4/27/2022 9 14 OK MW-14 Beryllium 4/18/2022 5/2/2022 14 180 OK MW-14 Bicarbonate as CaC03 4/18/2022 4/23/2022 5 14 OK MW-14 Cadmium 4/18/2022 5/2/2022 14 180 OK MW-14 Calcium 4/18/2022 5/2/2022 14 180 OK MW-14 Carbon Tetrachloride 4/18/2022 4/27/2022 9 14 OK MW-14 Carbonate as C03 4/18/2022 4/23/2022 5 14 OK MW-14 Chloride 4/18/2022 5/2/2022 14 28 OK MW-14 Chloroform 4/18/2022 4/27/2022 9 14 OK MW-14 Chloromethane 4/18/2022 4/27/2022 9 14 OK MW-14 Chromium 4/18/2022 5/2/2022 14 180 OK MW-14 Cobalt 4/18/2022 5/2/2022 14 180 OK MW-14 Copper 4/18/2022 5/2/2022 14 180 OK MW-14 Fluoride 4/18/2022 5/2/2022 14 28 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-14 Gross Radium Alpha 4/18/2022 5/18/2022 30 180 OK MW-14 Iron 4/18/2022 5/2/2022 14 180 OK MW-14 Lead 4/18/2022 5/2/2022 14 180 OK MW-14 Magnesium 4/18/2022 5/2/2022 14 180 OK MW-14 Manganese 4/18/2022 5/2/2022 14 180 OK MW-14 Mercury 4/18/2022 5/3/2022 15 180 OK MW-14 Methyl Ethyl Ketone 4/18/2022 4/27/2022 9 14 OK MW-14 Methylene Chloride 4/18/2022 4/27/2022 9 14 OK MW-14 Molybdenum 4/18/2022 5/2/2022 14 180 OK MW-14 Naphthalene 4/18/2022 4/27/2022 9 14 OK MW-14 Nickel 4/18/2022 5/2/2022 14 180 OK MW-14 Nitrate + Nitrite as N 4/18/2022 4/25/2022 7 28 OK MW-14 Nitrogen, Ammonia as N 4/18/2022 5/5/2022 17 28 OK MW-14 Potassium 4/18/2022 5/2/2022 14 180 OK MW-14 Selenium 4/18/2022 5/2/2022 14 180 OK MW-14 Silver 4/18/2022 5/2/2022 14 180 OK MW-14 Sodium 4/18/2022 5/2/2022 14 180 OK MW-14 Sulfate 4/18/2022 4/27/2022 9 28 OK MW-14 Te1rahydrofuran 4/18/2022 4/27/2022 9 14 OK MW-14 Thallium 4/18/2022 5/2/2022 14 180 OK MW-14 Tin 4/18/2022 5/2/2022 14 180 OK MW-14 Toluene 4/18/2022 4/27/2022 9 14 OK MW-14 Total Dissolved Solids 4/18/2022 4/25/2022 7 7 OK MW-14 Uranium 4/18/2022 5/17/2022 29 180 OK MW-14 Vanadium 4/18/2022 5/2/2022 14 180 OK MW-14 Xvlenes total 4/18/2022 4/27/2022 9 14 OK MW-14 Zinc 4/18/2022 5/2/2022 14 180 OK MW-15 Acetone 4/19/2022 4/27/2022 8 14 OK MW-15 Arsenic 4/19/2022 5/2/2022 13 180 OK MW-15 Benzene 4/19/2022 4/27/2022 8 14 OK MW-15 Beryllium 4/19/2022 5/2/2022 13 180 OK MW-15 Bicarbonate as CaC03 4/19/2022 4/23/2022 4 14 OK MW-15 Cadmium 4/19/2022 5/2/2022 13 180 OK MW-15 Calcium 4/19/2022 5/2/2022 13 180 OK MW-15 Carbon Tetrachloride 4/19/2022 4/27/2022 8 14 OK MW-15 Carbonate as C03 4/19/2022 4/23/2022 4 14 OK MW-15 Chloride 4/19/2022 5/2/2022 13 28 OK MW-15 Chloroform 4/19/2022 4/27/2022 8 14 OK MW-15 Chloromethane 4/19/2022 4/27/2022 8 14 OK MW-15 Chromium 4/19/2022 5/2/2022 13 180 OK MW-15 Cobalt 4/19/2022 5/2/2022 13 180 OK MW-15 Copper 4/19/2022 5/2/2022 13 180 OK MW-15 Fluoride 4/19/2022 5/2/2022 13 28 OK MW-15 Gross Radium Alpha 4/19/2022 5/18/2022 29 180 OK MW-15 Iron 4/19/2022 5/2/2022 13 180 OK MW-15 Lead 4/19/2022 5/2/2022 13 180 OK MW-15 Mag-nesium 4/19/2022 5/2/2022 13 180 OK MW-15 Manganese 4/19/2022 5/2/2022 13 180 OK MW-15 Mercury 4/19/2022 5/3/2022 14 180 OK MW-15 Methyl E1hyl Ketone 4/19/2022 4/27/2022 8 14 OK MW-15 Methylene Chloride 4/19/2022 4/27/2022 8 14 OK MW-15 Molybdenum 4/19/2022 5/2/2022 13 180 OK MW-15 Naphthalene 4/19/2022 4/27/2022 8 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-15 Nickel 4/19/2022 5/2/2022 13 180 OK MW-15 Nitrate + Nitrite as N 4/19/2022 4/25/2022 6 28 OK MW-15 Nitrogen, Ammonia as N 4/19/2022 5/5/2022 16 28 OK MW-15 Potassium 4/19/2022 5/2/2022 13 180 OK MW-15 Selenium 4/19/2022 5/2/2022 13 180 OK MW-15 Silver 4/19/2022 5/2/2022 13 180 OK MW-15 Sodium 4/19/2022 5/2/2022 13 180 OK MW-15 Sulfate 4/19/2022 4/27/2022 8 28 OK MW-15 Tetrah ydrnfu ran 4/19/2022 4/27/2022 8 14 OK MW-15 Thallium 4/19/2022 5/2/2022 13 180 OK MW-15 Tin 4/19/2022 5/2/2022 13 180 OK MW-15 Toluene 4/19/2022 4/27/2022 8 14 OK MW-15 Total Dissolved Solids 4/19/2022 4/25/2022 6 7 OK MW-15 Uranium 4/19/2022 5/2/2022 13 180 OK MW-15 Vanadium 4/19/2022 5/2/2022 13 180 OK MW-15 Xylenes, total 4/19/2022 4/27/2022 8 14 OK MW-15 Zinc 4/19/2022 5/2/2022 13 180 OK MW-17 Acetone 4/18/2022 4/27/2022 9 14 OK MW-17 Arsenic 4/18/2022 5/2/2022 14 180 OK MW-17 Benzene 4/18/2022 4/27/2022 9 14 OK MW-17 Beryllium 4/18/2022 5/2/2022 14 180 OK MW-17 Bicarbonate as CaC03 4/18/2022 4/23/2022 5 14 OK MW-17 Cadmium 4/18/2022 5/2/2022 14 180 OK MW-17 Calcium 4/18/2022 5/2/2022 14 180 OK MW-17 Carbon Tetrachloride 4/18/2022 4/27/2022 9 14 OK MW-17 Carbonate as C03 4/18/2022 4/23/2022 5 14 OK MW-17 Chloride 4/18/2022 5/2/2022 14 28 OK MW-17 Chloroform 4/18/2022 4/27/2022 9 14 OK MW-17 Chloromethane 4/18/2022 4/27/2022 9 14 OK MW-17 Chromium 4/18/2022 5/2/2022 14 180 OK MW-17 Cobalt 4/18/2022 5/2/2022 14 180 OK MW-17 Copper 4/18/2022 5/2/2022 14 180 OK MW-17 Fluoride 4/18/2022 5/2/2022 14 28 OK MW-17 Gross Radium Alpha 4/18/2022 5/18/2022 30 180 OK MW-17 Iron 4/18/2022 5/2/2022 14 180 OK MW-17 Lead 4/18/2022 5/2/2022 14 180 OK MW-17 Magnesium 4/18/2022 5/2/2022 14 180 OK MW-17 Manganese 4/18/2022 5/2/2022 14 180 OK MW-17 Mercury 4/18/2022 5/3/2022 15 180 OK MW-17 Methyl Ethyl Ketone 4/18/2022 4/27/2022 9 14 OK MW-17 Methylene Chloride 4/18/2022 4/27/2022 9 14 OK MW-17 Molybdenum 4/18/2022 5/2/2022 14 180 OK MW-17 Naphthalene 4/18/2022 4/27/2022 9 14 OK MW-17 Nickel 4/18/2022 5/2/2022 14 180 OK MW-17 Nitrate + Nitrite as N 4/18/2022 4/25/2022 7 28 OK MW-17 Nitrogen, Ammonia as N 4/18/2022 5/5/2022 17 28 OK MW-17 Potassium 4/18/2022 5/2/2022 14 180 OK MW-17 Selenium 4/18/2022 5/2/2022 14 180 OK MW-17 Silver 4/18/2022 5/2/2022 14 180 OK MW-17 Sodium 4/18/2022 5/2/2022 14 180 OK MW-17 Sulfate 4/18/2022 4/27/2022 9 28 OK MW-17 Tetrahydrofuran 4/18/2022 4/27/2022 9 14 OK MW-17 Thallium 4/18/2022 5/2/2022 14 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-17 Tin 4/18/2022 5/2/2022 14 180 OK MW-17 Toluene 4/18/2022 4/27/2022 9 14 OK MW-17 Total Dissolved Solids 4/18/2022 4/25/2022 7 7 OK MW-17 Uranium 4/18/2022 5/2/2022 14 180 OK MW-17 Vanadium 4/18/2022 5/2/2022 14 180 OK MW-17 Xylenes, total 4/18/2022 4/27/2022 9 14 OK MW-17 Zinc 4/18/2022 5/2/2022 14 180 OK MW-18 Acetone 4/13/2022 4/25/2022 12 14 OK MW-18 Arsenic 4/13/2022 4/26/2022 13 180 OK MW-18 Benzene 4/13/2022 4/25/2022 12 14 OK MW-18 Beryllium 4/13/2022 4/26/2022 13 180 OK MW-18 Bicarbonate as CaC03 4/13/2022 4/16/2022 3 14 OK MW-18 Cadmium 4/13/2022 4/26/2022 13 180 OK MW-18 Calcium 4/13/2022 4/27/2022 14 180 OK MW-18 Carbon Tetrachloride 4/13/2022 4/25/2022 12 14 OK MW-18 Carbonate as C03 4/13/2022 4/16/2022 3 14 OK MW-18 Chloride 4/13/2022 4/19/2022 6 28 OK MW-18 Chloroform 4/13/2022 4/25/2022 12 14 OK MW-18 Chloromethane 4/13/2022 4/25/2022 12 14 OK MW-18 Chromium 4/13/2022 4/26/2022 13 180 OK MW-18 Cobalt 4/13/2022 4/26/2022 13 180 OK MW-18 Copper 4/13/2022 4/26/2022 13 180 OK MW-18 Fluoride 4/13/2022 5/4/2022 21 28 OK MW-18 Gross Radium Alpha 4/13/2022 5/10/2022 27 180 OK MW-18 Iron 4/13/2022 4/27/2022 14 180 OK MW-18 Lead 4/13/2022 4/26/2022 13 180 OK MW-18 Magnesium 4/13/2022 4/27/2022 14 180 OK MW-18 Manganese 4/13/2022 4/26/2022 13 180 OK MW-18 Mercury 4/13/2022 4/26/2022 13 180 OK MW-18 Methyl Ethyl Ketone 4/13/2022 4/25/2022 12 14 OK MW-18 Me1J1ylene Chloride 4/13/2022 4/25/2022 12 14 OK MW-18 Molybdenum 4/13/2022 4/26/2022 13 180 OK MW-18 Naphthalene 4/13/2022 4/25/2022 12 14 OK MW-18 Nickel 4/13/2022 4/26/2022 13 180 OK MW-18 Nitrate+ Nitrite as N 4/13/2022 4/21/2022 8 28 OK MW-18 Nitrogen, Ammonia as N 4/13/2022 5/5/2022 22 28 OK MW-18 Potassium 4/13/2022 4/27/2022 14 180 OK MW-18 Selenium 4/13/2022 4/26/2022 13 180 OK MW-18 Silver 4/13/2022 4/26/2022 13 180 OK MW-18 Sodium 4/13/2022 4/27/2022 14 180 OK MW-18 Sulfate 4/13/2022 4/19/2022 6 28 OK MW-18 Tetrahydrofuran 4/13/2022 4/25/2022 12 14 OK MW-18 Thallium 4/13/2022 4/26/2022 13 180 OK MW-18 Tin 4/13/2022 4/27/2022 14 180 OK MW-18 Toluene 4/13/2022 4/25/2022 12 14 OK MW-18 Total Dissolved Solids 4/13/2022 4/18/2022 5 7 OK MW-18 Uranium 4/13/2022 4/26/2022 13 180 OK MW-18 Vanadium 4/13/2022 4/26/2022 13 180 OK MW-18 Xylenes, total 4/13/2022 4/25/2022 12 14 OK MW-18 Zinc 4/13/2022 4/26/2022 13 180 OK MW-19 Acetone 4/13/2022 4/26/2022 13 14 OK MW-19 Arsenic 4/13/2022 4/26/2022 13 180 OK MW-19 Benzene 4/13/2022 4/26/2022 13 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-19 Beryllium 4/13/2022 4/26/2022 13 180 OK MW-19 Bicarbonate as CaC03 4/13/2022 4/16/2022 3 14 OK MW-19 Cadmium 4/13/2022 4/26/2022 13 180 OK MW-19 Calcium 4/13/2022 4/27/2022 14 180 OK MW-19 Carbon Tetrachloride 4/13/2022 4/26/2022 13 14 OK MW-19 Carbonate as C03 4/13/2022 4/16/2022 3 14 OK MW-19 Chloride 4/13/2022 4/19/2022 6 28 OK MW-19 Chloroform 4/13/2022 4/26/2022 13 14 OK MW-19 Chloromethane 4/13/2022 4/26/2022 13 14 OK MW-19 Chromium 4/13/2022 4/26/2022 13 180 OK MW-19 Cobalt 4/13/2022 4/26/2022 13 180 OK MW-19 Coooer 4/13/2022 4/26/2022 13 180 OK MW-19 Fluoride 4/13/2022 4/19/2022 6 28 OK MW-19 Gross Radium Alpha 4/13/2022 5/10/2022 27 180 OK MW-19 Iron 4/13/2022 4/27/2022 14 180 OK MW-19 Lead 4/13/2022 4/26/2022 13 180 OK MW-19 Magnesium 4/13/2022 4/27/2022 14 180 OK MW-19 Manganese 4/13/2022 4/26/2022 13 180 OK MW-19 Mercury 4/13/2022 4/26/2022 13 180 OK MW-19 Methyl Ethyl Ketone 4/13/2022 4/26/2022 13 14 OK MW-19 Methylene Chloride 4/13/2022 4/26/2022 13 14 OK MW-19 Molybdenum 4/13/2022 4/26/2022 13 180 OK MW-19 Naphthalene 4/13/2022 4/26/2022 13 14 OK MW-19 Nickel 4/13/2022 4/26/2022 13 180 OK MW-19 Nitrate + Nitrite as N 4/13/2022 4/21/2022 8 28 OK MW-19 Nitrogen, Ammonia as N 4/13/2022 5/5/2022 22 28 OK MW-19 Potassium 4/13/2022 4/27/2022 14 180 OK MW-19 Selenium 4/13/2022 4/26/2022 13 180 OK MW-19 Silver 4/13/2022 4/26/2022 13 180 OK MW-19 Sodium 4/13/2022 4/27/2022 14 180 OK MW-19 Sulfate 4/13/2022 4/19/2022 6 28 OK MW-19 Telrahydrofuran 4/13/2022 4/26/2022 13 14 OK MW-19 Thallium 4/13/2022 4/26/2022 13 180 OK MW-19 Tin 4/13/2022 4/27/2022 14 180 OK MW-19 Toluene 4/13/2022 4/26/2022 13 14 OK MW-19 Total Dissolved Solids 4/13/2022 4/18/2022 5 7 OK MW-19 Uranium 4/13/2022 4/26/2022 13 180 OK MW-19 Vanadium 4/13/2022 4/26/2022 13 180 OK MW-19 Xylenes, total 4/13/2022 4/26/2022 13 14 OK MW-19 Zinc 4/13/2022 4/26/2022 13 180 OK MW-20 Acetone 5/17/2022 5/25/2022 8 14 OK MW-20 Arsenic 5/17/2022 5/27/2022 IO 180 OK MW-20 Benzene 5/17/2022 5/25/2022 8 14 OK MW-20 Beryllium 5/17/2022 5/27/2022 IO 180 OK MW-20 Bicarbonate as CaC03 5/17/2022 5/24/2022 7 14 OK MW-20 Cadmium 5/17/2022 5/27/2022 IO 180 OK MW-20 Calcium 5/17/2022 5/27/2022 IO 180 OK MW-20 Carbon Tetrachloride 5/17/2022 5/25/2022 8 14 OK MW-20 Carbonate as C03 5/17/2022 5/24/2022 7 14 OK MW-20 Chloride 5/17/2022 5/25/2022 8 28 OK MW-20 Chloroform 5/17/2022 5/25/2022 8 14 OK MW-20 Chloromethane 5/17/2022 5/25/2022 8 14 OK MW-20 Chromium 5/17/2022 5/27/2022 10 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-20 Cobalt 5/17/2022 5/27/2022 10 180 OK MW-20 Coooer 5/17/2022 5/27/2022 10 180 OK MW-20 Fluoride 5/17/2022 5/25/2022 8 28 OK MW-20 Gross Radium Alpha 5/17/2022 5/24/2022 7 180 OK MW-20 Iron 5/17/2022 5/27/2022 10 180 OK MW-20 Lead 5/17/2022 5/27/2022 10 180 OK MW-20 Magnesium 5/17/2022 5/27/2022 10 180 OK MW-20 Manganese 5/17/2022 5/27/2022 10 180 OK MW-20 Mercury 5/17/2022 5/20/2022 3 180 OK MW-20 Methyl Ethyl Ketone 5/17/2022 5/25/2022 8 14 OK MW-20 Methylene Chloride 5/17/2022 5/25/2022 8 14 OK MW-20 Molybdenum 5/17/2022 5/27/2022 10 180 OK MW-20 NaphLhalene 5/17/2022 5/25/2022 8 14 OK MW-20 Nickel 5/17/2022 5/27/2022 10 180 OK MW-20 Nitrate + Nitrite as N 5/17/2022 5/24/2022 7 28 OK MW-20 Nitroe.en, Ammonia as N 5/17/2022 5/27/2022 10 28 OK MW-20 Potassium 5/17/2022 5/27/2022 10 180 OK MW-20 Selenium 5/17/2022 5/27/2022 10 180 OK MW-20 Silver 5/17/2022 5/27/2022 10 180 OK MW-20 Sodium 5/17/2022 5/27/2022 10 180 OK MW-20 Sulfate 5/17/2022 5/31/2022 14 28 OK MW-20 Tetrahydrofuran 5/17/2022 5/25/2022 8 14 OK MW-20 Thallium 5/17/2022 5/27/2022 10 180 OK MW-20 Tin 5/17/2022 5/27/2022 10 180 OK MW-20 Toluene 5/17/2022 5/25/2022 8 14 OK MW-20 Total Dissolved Solids 5/17/2022 5/19/2022 2 7 OK MW-20 Uranium 5/17/2022 5/27/2022 10 180 OK MW-20 Vanadium 5/17/2022 5/27/2022 10 180 OK MW-20 Xylenes, total 5/17/2022 5/25/2022 8 14 OK MW-20 Zinc 5/17/2022 5/27/2022 10 180 OK MW-22 Acetone 4/25/2022 5/3/2022 8 14 OK MW-22 Arsenic 4/25/2022 5/10/2022 15 180 OK MW-22 Benzene 4/25/2022 5/3/2022 8 14 OK MW-22 Beryllium 4/25/2022 5/10/2022 15 180 OK MW-22 Bicarbonate as CaC03 4/25/2022 5/3/2022 8 14 OK MW-22 Cadmium 4/25/2022 5/10/2022 15 180 OK MW-22 Calcium 4/25/2022 5/10/2022 15 180 OK MW-22 Carbon Tetrachloride 4/25/2022 5/3/2022 8 14 OK MW-22 Carbonate as C03 4/25/2022 5/3/2022 8 14 OK MW-22 Chloride 4/25/2022 5/8/2022 13 28 OK MW-22 Chloroform 4/25/2022 5/3/2022 8 14 OK MW-22 Chloromethane 4/25/2022 5/3/2022 8 14 OK MW-22 Chromium 4/25/2022 5/10/2022 15 180 OK MW-22 Cobalt 4/25/2022 5/10/2022 15 180 OK MW-22 Copper 4/25/2022 5/10/2022 15 180 OK MW-22 Fluoride 4/25/2022 5/4/2022 9 28 OK MW-22 Gross Radium Alpha 4/25/2022 5/24/2022 29 180 OK MW-22 Iron 4/25/2022 5/11/2022 16 180 OK MW-22 Lead 4/25/2022 5/10/2022 15 180 OK MW-22 Magnesium 4/25/2022 5/11/2022 16 180 OK MW-22 Manganese 4/25/2022 5/10/2022 15 180 OK MW-22 Mercury 4/25/2022 5/4/2022 9 180 OK MW-22 Methyl Ethyl Ketone 4/25/2022 5/3/2022 8 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-22 Methylene Chloride 4/25/2022 5/3/2022 8 14 OK MW-22 Molybdenum 4/25/2022 5/10/2022 15 180 OK MW-22 Naphthalene 4/25/2022 5/3/2022 8 14 OK MW-22 Nickel 4/25/2022 5/10/2022 15 180 OK MW-22 Nitrate + Nitrite as N 4/25/2022 4/30/2022 5 28 OK MW-22 Nitrogen, Ammonia as N 4/25/2022 5/12/2022 17 28 OK MW-22 Potassium 4/25/2022 5/11/2022 16 180 OK MW-22 Selenium 4/25/2022 5/10/2022 15 180 OK MW-22 Silver 4/25/2022 5/10/2022 15 180 OK MW-22 Sodium 4/25/2022 5/11/2022 16 180 OK MW-22 Sulfate 4/25/2022 5/8/2022 13 28 OK MW-22 Tetrahydrofuran 4/25/2022 5/3/2022 8 14 OK MW-22 Thallium 4/25/2022 5/10/2022 15 180 OK MW-22 Tin 4/25/2022 5/11/2022 16 180 OK MW-22 Toluene 4/25/2022 5/3/2022 8 14 OK MW-22 Total Dissolved Solids 4/25/2022 5/2/2022 7 7 OK MW-22 Uranium 4/25/2022 5/10/2022 15 180 OK MW-22 Vanadium 4/25/2022 5/10/2022 15 180 OK MW-22 X y!enes, total 4/25/2022 5/3/2022 8 14 OK MW-22 Zinc 4/25/2022 5/10/2022 15 180 OK MW-23 Acetone 4/27/2022 5/3/2022 6 14 OK MW-23 Arsenic 4/27/2022 5/10/2022 13 180 OK MW-23 Benzene 4/27/2022 5/3/2022 6 14 OK MW-23 Beryllium 4/27/2022 5/10/2022 13 180 OK MW-23 Bicarbonate as CaC03 4/27/2022 5/3/2022 6 14 OK MW-23 Cadmium 4/27/2022 5/10/2022 13 180 OK MW-23 Calcium 4/27/2022 5/10/2022 13 180 OK MW-23 Carbon Tetrachloride 4/27/2022 5/3/2022 6 14 OK MW-23 Carbonate as C03 4/27/2022 5/3/2022 6 14 OK MW-23 Chloride 4/27/2022 5/9/2022 12 28 OK MW-23 Chloroform 4/27/2022 5/3/2022 6 14 OK MW-23 Chloromethane 4/27/2022 5/3/2022 6 14 OK MW-23 Chromium 4/27/2022 5/10/2022 13 180 OK MW-23 Cobalt 4/27/2022 5/10/2022 13 180 OK MW-23 Coooer 4/27/2022 5/10/2022 13 180 OK MW-23 Fluoride 4/27/2022 5/4/2022 7 28 OK MW-23 Gross Radium Alpha 4/27/2022 5/24/2022 27 180 OK MW-23 Iron 4/27/2022 5/10/2022 13 180 OK MW-23 Lead 4/27/2022 5/10/2022 13 180 OK MW-23 Magnesium 4/27/2022 5/10/2022 13 180 OK MW-23 Manganese 4/27/2022 5/10/2022 13 180 OK MW-23 Mercury 4/27/2022 5/4/2022 7 180 OK MW-23 Methyl Ethyl Ketone 4/27/2022 5/3/2022 6 14 OK MW-23 Methylene Chloride 4/27/2022 5/3/2022 6 14 OK MW-23 Molybdenum 4/27/2022 5/10/2022 13 180 OK MW-23 Naphthalene 4/27/2022 5/3/2022 6 14 OK MW-23 Nickel 4/27/2022 5/10/2022 13 180 OK MW-23 Nitrate + Nitrite as N 4/27/2022 4/30/2022 3 28 OK MW-23 Nitrogen, Ammonia as N 4/27/2022 5/12/2022 15 28 OK MW-23 Potassium 4/27/2022 5/10/2022 13 180 OK MW-23 Selenium 4/27/2022 5/10/2022 13 180 OK MW-23 Silver 4/27/2022 5/10/2022 13 180 OK MW-23 Sodium 4/27/2022 5/11/2022 14 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-23 Sulfate 4/27/2022 5/8/2022 11 28 OK MW-23 Tetrahydrofuran 4/27/2022 5/3/2022 6 14 OK MW-23 Thallium 4/27/2022 5/10/2022 13 180 OK MW-23 Tin 4/27/2022 5/10/2022 13 180 OK MW-23 Toluene 4/27/2022 5/3/2022 6 14 OK MW-23 Total Dissolved Solids 4/27/2022 5/2/2022 5 7 OK MW-23 Uranium 4/27/2022 5/10/2022 13 180 OK MW-23 Vanadium 4/27/2022 5/10/2022 13 180 OK MW-23 X vlenes, total 4/27/2022 5/3/2022 6 14 OK MW-23 Zinc 4/27/2022 5/10/2022 13 180 OK MW-24 Acetone 4/27/2022 5/3/2022 6 14 OK MW-24 Arsenic 4/27/2022 5/10/2022 13 180 OK MW-24 Benzene 4/27/2022 5/3/2022 6 14 OK MW-24 Beryllium 4/27/2022 5/10/2022 13 180 OK MW-24 Bicarbonate as CaC03 4/27/2022 5/3/2022 6 14 OK MW-24 Cadmium 4/27/2022 5/10/2022 13 180 OK MW-24 Calcium 4/27/2022 5/10/2022 13 180 OK MW-24 Carbon Tetrachloride 4/27/2022 5/3/2022 6 14 OK MW-24 Carbonate as C03 4/27/2022 5/3/2022 6 14 OK MW-24 Chloride 4/27/2022 5/9/2022 12 28 OK MW-24 Chloroform 4/27/2022 5/3/2022 6 14 OK MW-24 Chloromethane 4/27/2022 5/3/2022 6 14 OK MW-24 Chromium 4/27/2022 5/10/2022 13 180 OK MW-24 Cobalt 4/27/2022 5/10/2022 13 180 OK MW-24 Copper 4/27/2022 5/10/2022 13 180 OK MW-24 Fluoride 4/27/2022 5/4/2022 7 28 OK MW-24 Gross Radium Alpha 4/27/2022 5/24/2022 27 180 OK MW-24 Iron 4/27/2022 5/11/2022 14 180 OK MW-24 Lead 4/27/2022 5/10/2022 13 180 OK MW-24 Magnesium 4/27/2022 5/11/2022 14 180 OK MW-24 Manganese 4/27/2022 5/10/2022 13 180 OK MW-24 Mercury 4/27/2022 5/4/2022 7 180 OK MW-24 Methyl Ethvl Ketone 4/27/2022 5/3/2022 6 14 OK MW-24 Methylene Chloride 4/27/2022 5/3/2022 6 14 OK MW-24 Molybdenum 4/27/2022 5/10/2022 13 180 OK MW-24 Naphthalene 4/27/2022 5/3/2022 6 14 OK MW-24 Nickel 4/27/2022 5/10/2022 13 180 OK MW-24 Nitrate+ Nitrite as N 4/27/2022 4/30/2022 3 28 OK MW-24 Nitrogen, Ammonia as N 4/27/2022 5/12/2022 15 28 OK MW-24 Potassium 4/27/2022 5/11/2022 14 180 OK MW-24 Selenium 4/27/2022 5/10/2022 13 180 OK MW-24 Silver 4/27/2022 5/10/2022 13 180 OK MW-24 Sodium 4/27/2022 5/11/2022 14 180 OK MW-24 Sulfate 4/27/2022 5/8/2022 11 28 OK MW-24 Tetrnhydrof-uran 4/27/2022 5/3/2022 6 14 OK MW-24 Thallium 4/27/2022 5/10/2022 13 180 OK MW-24 Tin 4/27/2022 5/10/2022 13 180 OK MW-24 Toluene 4/27/2022 5/3/2022 6 14 OK MW-24 Total Dissolved Solids 4/27/2022 5/2/2022 5 7 OK MW-24 Uranium 4/27/2022 5/10/2022 13 180 OK MW-24 Vanadium 4/27/2022 5/10/2022 13 180 OK MW-24 Xylenes, total 4/27/2022 5/3/2022 6 14 OK MW-24 Zinc 4/27/2022 5/10/2022 13 180 OK G-2A: Quarterly Holding Time Evaluation I Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-24A Acetone 4/27/2022 5/3/2022 6 14 OK MW-24A Arsenic 4/27/2022 5/10/2022 13 180 OK MW-24A Benzene 4/27/2022 5/3/2022 6 14 OK MW-24A Beryllium 4/27/2022 5/10/2022 13 180 OK MW-24A Bicarbonate as CaC03 4/27/2022 5/4/2022 7 14 OK MW-24A Cadmium 4/27/2022 5/10/2022 13 180 OK MW-24A Calcium 4/27/2022 5/10/2022 13 180 OK MW-24A Carbon Tetrachloride 4/27/2022 5/3/2022 6 14 OK MW-24A Carbonate as C03 4/27/2022 5/4/2022 7 14 OK MW-24A Chloride 4/27/2022 5/9/2022 12 28 OK MW-24A Chloroform 4/27/2022 5/3/2022 6 14 OK MW-24A Chloromethane 4/27/2022 5/3/2022 6 14 OK MW-24A Chromium 4/27/2022 5/10/2022 13 180 OK MW-24A Cobalt 4/27/2022 5/10/2022 13 180 OK MW-24A Copper 4/27/2022 5/10/2022 13 180 OK MW-24A Fluoride 4/27/2022 5/4/2022 7 28 OK MW-24A Gross Radium Alpha 4/27/2022 5/24/2022 27 180 OK MW-24A Iron 4/27/2022 5/11/2022 14 180 OK MW-24A Lead 4/27/2022 5/10/2022 13 180 OK MW-24A Magnesium 4/27/2022 5/11/2022 14 180 OK MW-24A Manganese 4/27/2022 5/10/2022 13 180 OK MW-24A Mercury 4/27/2022 5/4/2022 7 180 OK MW-24A Methyl Ethyl Ketone 4/27/2022 5/3/2022 6 14 OK MW-24A Methylene Chloride 4/27/2022 5/3/2022 6 14 OK MW-24A Molybdenum 4/27/2022 5/10/2022 13 180 OK MW-24A Naphthalene 4/27/2022 5/3/2022 6 14 OK MW-24A Nickel 4/27/2022 5/10/2022 13 180 OK MW-24A Nitrate + Nitrite as N 4/27/2022 4/30/2022 3 28 OK MW-24A Nitrogen, Ammonia as N 4/27/2022 5/12/2022 15 28 OK MW-24A Potassium 4/27/2022 5/11/2022 14 180 OK MW-24A Selenium 4/27/2022 5/10/2022 13 180 OK MW-24A Silver 4/27/2022 5/10/2022 13 180 OK MW-24A Sodium 4/27/2022 5/11/2022 14 180 OK MW-24A Sulfate 4/27/2022 5/8/2022 11 28 OK MW-24A Tetrahydrofuran 4/27/2022 5/3/2022 6 14 OK MW-24A Thallium 4/27/2022 5/10/2022 13 180 OK MW-24A Tin 4/27/2022 5/10/2022 13 180 OK MW-24A Toluene 4/27/2022 5/3/2022 6 14 OK MW-24A Total Dissolved Solids 4/27/2022 5/2/2022 5 7 OK MW-24A Uranium 4/27/2022 5/10/2022 13 180 OK MW-24A Vanadium 4/27/2022 5/10/2022 13 180 OK MW-24A Xylenes. total 4/27/2022 5/3/2022 6 14 OK MW-24A Zinc 4/27/2022 5/10/2022 13 180 OK MW-25 Acetone 4/12/2022 4/25/2022 13 14 OK MW-25 Arsenic 4/12/2022 4/26/2022 14 180 OK MW-25 Benzene 4/12/2022 4/25/2022 13 14 OK MW-25 Beryllium 4/12/2022 4/26/2022 14 180 OK MW-25 Bicarbonate as CaC03 4/12/2022 4/16/2022 4 14 OK MW-25 Cadmium 4/12/2022 4/26/2022 14 180 OK MW-25 Calcium 4/12/2022 4/27/2022 15 180 OK MW-25 Carbon Tetrachloride 4/12/2022 4/25/2022 13 14 OK MW-25 Carbonate as C03 4/12/2022 4/16/2022 4 14 OK MW-25 Chloride 4/12/2022 4/19/2022 7 28 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-25 Chloroform 4/12/2022 4/25/2022 13 14 OK MW-25 Chloromethane 4/12/2022 4/25/2022 13 14 OK MW-25 Chromium 4/12/2022 4/26/2022 14 180 OK MW-25 Cobalt 4/12/2022 4/26/2022 14 180 OK MW-25 Copper 4/12/2022 4/26/2022 14 180 OK MW-25 Fluoride 4/12/2022 5/4/2022 22 28 OK MW-25 Gross Radium Alpha 4/12/2022 5/10/2022 28 180 OK MW-25 Iron 4/12/2022 4/27/2022 15 180 OK MW-25 Lead 4/12/2022 4/26/2022 14 180 OK MW-25 Magnesium 4/12/2022 4/27/2022 15 180 OK MW-25 Manganese 4/12/2022 4/26/2022 14 180 OK MW-25 Mercury 4/12/2022 4/26/2022 14 180 OK MW-25 Methyl Ethyl Ketone 4/12/2022 4/25/2022 13 14 OK MW-25 Methylene Chloride 4/12/2022 4/25/2022 13 14 OK MW-25 Molybdenum 4/12/2022 4/26/2022 14 180 OK MW-25 Naphthalene 4/12/2022 4/25/2022 13 14 OK MW-25 Nickel 4/12/2022 4/26/2022 14 180 OK MW-25 Nitrate + Nitrite as N 4/12/2022 4/21/2022 9 28 OK MW-25 Nitrogen, Ammonia as N 4/12/2022 4/25/2022 13 28 OK MW-25 Potassium 4/12/2022 4/27/2022 15 180 OK MW-25 Selenium 4/12/2022 4/26/2022 14 180 OK -MW-25 Silver 4/12/2022 4/26/2022 14 180 OK MW-25 Sodium 4/12/2022 4/27/2022 15 180 OK MW-25 Sulfate 4/12/2022 4/19/2022 7 28 OK MW-25 Tetrahydrofuran 4/12/2022 4/25/2022 13 14 OK MW-25 Thallium 4/12/2022 4/26/2022 14 180 OK MW-25 Tin 4/12/2022 4/27/2022 15 180 OK MW-25 Toluene 4/12/2022 4/25/2022 13 14 OK MW-25 Total Dissolved Solids 4/12/2022 4/18/2022 6 7 OK MW-25 Uranium 4/12/2022 4/26/2022 14 180 OK MW-25 Vanadium 4/12/2022 4/26/2022 14 180 OK MW-25 Xylenes, total 4/12/2022 4/25/2022 13 14 OK MW-25 Zinc 4/12/2022 4/26/2022 14 180 OK MW-26 Acetone 4/20/2022 4/26/2022 6 14 OK MW-26 Arsenic 4/20/2022 5/2/2022 12 180 OK MW-26 Benzene 4/20/2022 4/26/2022 6 14 OK MW-26 Beryllium 4/20/2022 5/2/2022 12 180 OK MW-26 Bicarbonate as CaC03 4/20/2022 4/23/2022 3 14 OK MW-26 Cadmium 4/20/2022 5/2/2022 12 180 OK MW-26 Calcium 4/20/2022 5/2/2022 12 180 OK MW-26 Carbon Tetrachloride 4/20/2022 4/26/2022 6 14 OK MW-26 Carbonate as C03 4/20/2022 4/23/2022 3 14 OK MW-26 Chloride 4/20/2022 4/27/2022 7 28 OK MW-26 Chloroform 4/20/2022 4/26/2022 6 14 OK MW-26 Chloromethane 4/20/2022 4/26/2022 6 14 OK MW-26 Chromium 4/20/2022 5/2/2022 12 180 OK MW-26 Cobalt 4/20/2022 5/2/2022 12 180 OK MW-26 Coooer 4/20/2022 5/2/2022 12 180 OK MW-26 Fluoride 4/20/2022 5/3/2022 13 28 OK MW-26 Iron 4/20/2022 5/2/2022 12 180 OK MW-26 Lead 4/20/2022 5/2/2022 12 180 OK MW-26 Magnesium 4/20/2022 5/2/2022 12 180 OK MW-26 Manganese 4/20/2022 5/2/2022 12 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-26 Mercury 4/20/2022 5/3/2022 13 180 OK MW-26 Methyl Ethyl Ketone 4/20/2022 4/26/2022 6 14 OK MW-26 Methylene Chloride 4/20/2022 4/26/2022 6 14 OK MW-26 Molybdenum 4/20/2022 5/2/2022 12 180 OK MW-26 Naphthalene 4/20/2022 4/26/2022 6 14 OK MW-26 Nickel 4/20/2022 5/2/2022 12 180 OK MW-26 Nitrate + Nitrite as N 4/20/2022 4/25/2022 5 28 OK MW-26 Nitrogen, Ammonia as N 4/20/2022 5/5/2022 15 28 OK MW-26 Potassium 4/20/2022 5/2/2022 12 180 OK MW-26 Selenium 4/20/2022 5/2/2022 12 180 OK MW-26 Silver 4/20/2022 5/2/2022 12 180 OK MW-26 Sodium 4/20/2022 5/2/2022 12 180 OK MW-26 Sulfate 4/20/2022 4/27/2022 7 28 OK MW-26 Tetrahydrofuran 4/20/2022 4/26/2022 6 14 OK MW-26 Thallium 4/20/2022 5/2/2022 12 180 OK MW-26 Tin 4/20/2022 5/2/2022 12 180 OK MW-26 Toluene 4/20/2022 4/26/2022 6 14 OK MW-26 Total Dissolved Solids 4/20/2022 4/25/2022 5 7 OK MW-26 Uranium 4/20/2022 5/2/2022 12 180 OK MW-26 Vanadium 4/20/2022 5/2/2022 12 180 OK MW-26 Xylenes, total 4/20/2022 4/26/2022 6 14 OK MW-26 Zinc 4/20/2022 5/2/2022 12 180 OK MW-26 Gross Radium Alpha 4/27/2022 5/24/2022 27 180 OK MW-27 Acetone 4/12/2022 4/25/2022 13 14 OK MW-27 Arsenic 4/12/2022 4/26/2022 14 180 OK MW-27 Benzene 4/12/2022 4/25/2022 13 14 OK MW-27 Beryllium 4/12/2022 4/26/2022 14 180 OK MW-27 Bicarbonate as CaC03 4/12/2022 4/16/2022 4 14 OK MW-27 Cadmium 4/12/2022 4/26/2022 14 180 OK MW-27 Calcium 4/12/2022 4/27/2022 15 180 OK MW-27 Carbon Tetrachloride 4/12/2022 4/25/2022 13 14 OK MW-27 Carbonate as C03 4/12/2022 4/16/2022 4 14 OK MW-27 Chloride 4/12/2022 4/19/2022 7 28 OK MW-27 Chloroform 4/12/2022 4/25/2022 13 14 OK MW-27 Chloromethane 4/12/2022 4/25/2022 13 14 OK MW-27 Chromium 4/12/2022 4/26/2022 14 180 OK MW-27 Cobalt 4/12/2022 4/26/2022 14 180 OK MW-27 Copper 4/12/2022 4/26/2022 14 180 OK MW-27 Fluoride 4/12/2022 4/19/2022 7 28 OK MW-27 Gross Radium Alpha 4/12/2022 5/10/2022 28 180 OK MW-27 Iron 4/12/2022 4/27/2022 15 180 OK MW-27 Lead 4/12/2022 4/26/2022 14 180 OK MW-27 Magnesium 4/12/2022 4/27/2022 15 180 OK MW-27 Manganese 4/12/2022 4/26/2022 14 180 OK MW-27 Mercury 4/12/2022 4/26/2022 14 180 OK MW-27 Methyl Ethyl Ketone 4/12/2022 4/25/2022 13 14 OK MW-27 Methylene Chloride 4/12/2022 4/25/2022 13 14 OK MW-27 Molybdenum 4/12/2022 4/26/2022 14 180 OK MW-27 Naphthalene 4/12/2022 4/25/2022 13 14 OK MW-27 Nickel 4/12/2022 4/26/2022 14 180 OK MW-27 Nitrate + Nitrite as N 4/12/2022 4/21/2022 9 28 OK MW-27 Nitrogen, Ammonia as N 4/12/2022 5/5/2022 23 28 OK MW-27 Potassium 4/12/2022 4/27/2022 15 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-27 Selenium 4/12/2022 4/26/2022 14 180 OK MW-27 Silver 4/12/2022 4/26/2022 14 180 OK MW-27 Sodium 4/12/2022 4/27/2022 15 180 OK MW-27 Sulfate 4/12/2022 4/19/2022 7 28 OK MW-27 Tetrahydrofuran 4/12/2022 4/25/2022 13 14 OK MW-27 Thallium 4/12/2022 4/26/2022 14 180 OK MW-27 Tin 4/12/2022 4/27/2022 15 180 OK MW-27 Toluene 4/12/2022 4/25/2022 13 14 OK MW-27 Uranium 4/12/2022 4/26/2022 14 180 OK MW-27 Vanadium 4/12/2022 4/26/2022 14 180 OK MW-27 Xylenes, total 4/12/2022 4/25/2022 13 14 OK MW-27 Zinc 4/12/2022 4/26/2022 14 180 OK MW-27 Total Dissolved Solids 5/16/2022 5/19/2022 3 7 OK MW-28 Acetone 4/19/2022 4/26/2022 7 14 OK MW-28 Arsenic 4/19/2022 5/2/2022 13 180 OK MW-28 Benzene 4/19/2022 4/26/2022 7 14 OK MW-28 Beryllium 4/19/2022 5/2/2022 13 180 OK MW-28 Bicarbonate as CaC03 4/19/2022 4/23/2022 4 14 OK MW-28 Cadmium 4/19/2022 5/2/2022 13 180 OK MW-28 Calcium 4/19/2022 5/2/2022 13 180 OK MW-28 Carbon Tetrachloride 4/19/2022 4/26/2022 7 14 OK MW-28 Carbonate as C03 4/19/2022 4/23/2022 4 14 OK MW-28 Chloride 4/19/2022 4/27/2022 8 28 OK MW-28 Chloroform 4/19/2022 4/26/2022 7 14 OK MW-28 Chloromethane 4/19/2022 4/26/2022 7 14 OK MW-28 Chromium 4/19/2022 5/2/2022 13 180 OK MW-28 Cobalt 4/19/2022 5/2/2022 13 180 OK MW-28 Coooer 4/19/2022 5/2/2022 13 180 OK MW-28 Fluoride 4/19/2022 5/2/2022 13 28 OK MW-28 Gross Radium Alpha 4/19/2022 5/18/2022 29 180 OK MW-28 Iron 4/19/2022 5/2/2022 13 180 OK MW-28 Lead 4/19/2022 5/2/2022 13 180 OK MW-28 Magnesium 4/19/2022 5/2/2022 13 180 OK MW-28 Manganese 4/19/2022 5/2/2022 13 180 OK MW-28 Mercury 4/19/2022 5/3/2022 14 180 OK MW-28 Methyl Ethyl Ketone 4/19/2022 4/26/2022 7 14 OK MW-28 Methylene Chloride 4/19/2022 4/26/2022 7 14 OK MW-28 Molybdenum 4/19/2022 5/2/2022 13 180 OK MW-28 Naphthalene 4/19/2022 4/26/2022 7 14 OK MW-28 Nickel 4/19/2022 5/2/2022 13 180 OK MW-28 Nitrate + Nitrite as N 4/19/2022 4/25/2022 6 28 OK MW-28 Nitrogen, Ammonia as N 4/19/2022 5/5/2022 16 28 OK MW-28 Potassium 4/19/2022 5/2/2022 13 180 OK MW-28 Selenium 4/19/2022 5/2/2022 13 180 OK MW-28 Silver 4/19/2022 5/2/2022 13 180 OK MW-28 Sodium 4/19/2022 5/2/2022 13 180 OK MW-28 Sulfate 4/19/2022 4/27/2022 8 28 OK MW-28 Tetrahydrofuran 4/19/2022 4/26/2022 7 14 OK MW-28 Thallium 4/19/2022 5/2/2022 13 180 OK MW-28 Tin 4/19/2022 5/2/2022 13 180 OK MW-28 Toluene 4/19/2022 4/26/2022 7 14 OK MW-28 Total Dissolved Solids 4/19/2022 4/25/2022 6 7 OK MW-28 Uranium 4/19/2022 5/2/2022 13 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time 1, Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-28 Vanadium 4/19/2022 5/2/2022 13 180 OK MW-28 X ylenes, total 4/19/2022 4/26/2022 7 14 OK MW-28 Zinc 4/19/2022 5/2/2022 13 180 OK MW-29 Acetone 4/14/2022 4/26/2022 12 14 OK MW-29 Arsenic 4/14/2022 4/26/2022 12 180 OK MW-29 Benzene 4/14/2022 4/26/2022 12 14 OK MW-29 Beryllium 4/14/2022 4/26/2022 12 180 OK MW-29 Bicarbonate as CaC03 4/14/2022 4/16/2022 2 14 OK MW-29 Cadmium 4/14/2022 4/26/2022 12 180 OK MW-29 Calcium 4/14/2022 4/27/2022 13 180 OK MW-29 Carbon Tetrachloride 4/14/2022 4/26/2022 12 14 OK MW-29 Carbonate as C03 4/14/2022 4/16/2022 2 14 OK MW-29 Chloride 4/14/2022 4/19/2022 5 28 OK MW-29 Chloroform 4/14/2022 4/26/2022 12 14 OK MW-29 Chloromethane 4/14/2022 4/26/2022 12 14 OK MW-29 Chromium 4/14/2022 4/26/2022 12 180 OK MW-29 Cobalt 4/14/2022 4/26/2022 12 180 OK MW-29 Copper 4/14/2022 4/26/2022 12 180 OK MW-29 Fluoride 4/14/2022 4/19/2022 5 28 OK MW-29 Gross Radium Alpha 4/14/2022 5/10/2022 26 180 OK MW-29 Iron 4/14/2022 4/27/2022 13 180 OK MW-29 Lead 4/14/2022 4/26/2022 12 180 OK MW-29 Magnesium 4/14/2022 4/27/2022 13 180 OK MW-29 Manganese 4/14/2022 4/26/2022 12 180 OK MW-29 Mercury 4/14/2022 4/26/2022 12 180 OK MW-29 Methyl Ethyl Ketone 4/14/2022 4/26/2022 12 14 OK MW-29 Methylene Chloride 4/14/2022 4/26/2022 12 14 OK MW-29 Molybdenum 4/14/2022 4/26/2022 12 180 OK MW-29 Naphthalene 4/14/2022 4/26/2022 12 14 OK MW-29 Nickel 4/14/2022 4/26/2022 12 180 OK MW-29 Nitrate + Nitrite as N 4/14/2022 4/21/2022 7 28 OK MW-29 Nitrogen, Ammonia as N 4/14/2022 4/25/2022 11 28 OK MW-29 Potassium 4/14/2022 4/27/2022 13 180 OK MW-29 Selenium 4/14/2022 4/26/2022 12 180 OK MW-29 Silver 4/14/2022 4/26/2022 12 180 OK MW-29 Sodium 4/14/2022 4/27/2022 13 180 OK MW-29 Sulfate 4/14/2022 4/19/2022 5 28 OK MW-29 Tetrahydrofuran 4/14/2022 4/26/2022 12 14 OK MW-29 Thallium 4/14/2022 4/26/2022 12 180 OK MW-29 Tin 4/14/2022 4/27/2022 13 180 OK MW-29 Toluene 4/14/2022 4/26/2022 12 14 OK MW-29 Total Dissolved Solids 4/14/2022 4/19/2022 5 7 OK MW-29 Uranium 4/14/2022 4/26/2022 12 180 OK MW-29 Vanadium 4/14/2022 4/26/2022 12 180 OK MW-29 Xylenes, total 4/14/2022 4/26/2022 12 14 OK MW-29 Zinc 4/14/2022 4/26/2022 12 180 OK MW-30 Acetone 4/20/2022 4/26/2022 6 14 OK MW-30 Arsenic 4/20/2022 5/2/2022 12 180 OK MW-30 Benzene 4/20/2022 4/26/2022 6 14 OK MW-30 Beryllium 4/20/2022 5/2/2022 12 180 OK MW-30 Bicarbonate as CaC03 4/20/2022 4/23/2022 3 14 OK MW-30 Cadmium 4/20/2022 5/2/2022 12 180 OK MW-30 Calcium 4/20/2022 5/2/2022 12 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-30 Carbon Tetrachloride 4/20/2022 4/26/2022 6 14 OK MW-30 Carbonate as C03 4/20/2022 4/23/2022 3 14 OK MW-30 Chloride 4/20/2022 4/27/2022 7 28 OK MW-30 Chloroform 4/20/2022 4/26/2022 6 14 OK MW-30 Chloromethane 4/20/2022 4/26/2022 6 14 OK MW-30 Chromium 4/20/2022 5/2/2022 12 180 OK MW-30 Cobalt 4/20/2022 5/2/2022 12 180 OK MW-30 Copper 4/20/2022 5/2/2022 12 180 OK MW-30 Fluoride 4/20/2022 5/3/2022 13 28 OK MW-30 Gross Radium Alpha 4/20/2022 5/18/2022 28 180 OK MW-30 Iron 4/20/2022 5/2/2022 12 180 OK MW-30 Lead 4/20/2022 5/2/2022 12 180 OK MW-30 Magnes.ium 4/20/2022 5/2/2022 12 180 OK MW-30 Manganese 4/20/2022 5/2/2022 12 180 OK MW-30 Mercury 4/20/2022 5/3/2022 13 180 OK MW-30 Methyl Ethyl Ketone 4/20/2022 4/26/2022 6 14 OK MW-30 Methylene Chloride 4/20/2022 4/26/2022 6 14 OK MW-30 Molvbdem11n 4/20/2022 5/2/2022 12 180 OK MW-30 Naphthalene 4/20/2022 4/26/2022 6 14 OK MW-30 Nickel 4/20/2022 5/2/2022 12 180 OK MW-30 Nitrate + Nitrite as N 4/20/2022 4/25/2022 5 28 OK MW-30 Nitrogen, Ammonia as N 4/20/2022 5/5/2022 15 28 OK MW-30 Potassium 4/20/2022 5/2/2022 12 180 OK MW-30 Selenium 4/20/2022 5/2/2022 12 180 OK MW-30 Silver 4/20/2022 5/2/2022 12 180 OK MW-30 Sodium 4/20/2022 5/2/2022 12 180 OK MW-30 Sulfate 4/20/2022 4/27/2022 7 28 OK MW-30 Tetrahydrofuran 4/20/2022 4/26/2022 6 14 OK MW-30 Thallium 4/20/2022 5/2/2022 12 180 OK MW-30 Tin 4/20/2022 5/2/2022 12 180 OK MW-30 Toluene 4/20/2022 4/26/2022 6 14 OK MW-30 Total Dissolved Solids 4/20/2022 4/25/2022 5 7 OK MW-30 Uranium 4/20/2022 5/2/2022 12 180 OK MW-30 Vanadium 4/20/2022 5/2/2022 12 180 OK MW-30 Xylenes, total 4/20/2022 4/26/2022 6 14 OK MW-30 Zinc 4/20/2022 5/2/2022 12 180 OK MW-31 Acetone 4/11/2022 4/25/2022 14 14 OK MW-31 Arsenic 4/11/2022 4/26/2022 15 180 OK MW-31 Benzene 4/11/2022 4/25/2022 14 14 OK MW-31 Beryllium 4/11/2022 4/26/2022 15 180 OK MW-31 Bicarbonate as CaC03 4/11/2022 4/16/2022 5 14 OK MW-31 Cadmium 4/11/2022 4/26/2022 15 180 OK MW-31 Calcium 4/11/2022 4/27/2022 16 180 OK MW-31 Carbon Tetrachloride 4/11/2022 4/25/2022 14 14 OK MW-31 Carbonate as C03 4/11/2022 4/16/2022 5 14 OK MW-31 Chloride 4/11/2022 4/19/2022 8 28 OK MW-31 Chloroform 4/11/2022 4/25/2022 14 14 OK MW-31 Chloromethane 4/11/2022 4/25/2022 14 14 OK MW-31 Chromium 4/11/2022 4/26/2022 15 180 OK MW-31 Cobalt 4/11/2022 4/26/2022 15 180 OK MW-31 Copper 4/11/2022 4/26/2022 15 180 OK MW-31 Fluoride 4/11/2022 4/18/2022 7 28 OK MW-31 Gross Radium Aloha 4/11/2022 5/10/2022 29 180 OK G-2A: Quarterly Holding Time Evaluation I• Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-31 Iron 4/11/2022 4/27/2022 16 180 OK MW-31 Lead 4/11/2022 4/26/2022 15 180 OK MW-31 Magnesium 4/11/2022 4/27/2022 16 180 OK MW-31 Manganese 4/11/2022 4/26/2022 ]5 180 OK MW-31 Mercury 4/11/2022 4/26/2022 15 180 OK MW-31 Methyl Ethyl Ketone 4/11/2022 4/25/2022 14 14 OK MW-31 Methylene Chloride 4/11/2022 4/25/2022 14 14 OK MW-31 Molybdenum 4/11/2022 4/26/2022 15 180 OK MW-31 Naphthalene 4/11/2022 4/25/2022 14 14 OK MW-31 Nickel 4/11/2022 4/26/2022 15 180 OK MW-31 Nitrate + Nitrite as N 4/11/2022 4/21/2022 10 28 OK MW-31 Nitrogen, Ammonia as N 4/11/2022 5/5/2022 24 28 OK MW-31 Potassium 4/11/2022 4/27/2022 16 180 OK MW-31 Selenium 4/11/2022 4/26/2022 15 180 OK MW-31 Silver 4/11/2022 4/26/2022 15 180 OK MW-31 Sodium 4/11/2022 4/27/2022 16 180 OK MW-31 Sulfate 4/11/2022 4/19/2022 8 28 OK MW-31 Tetrahydrofuran 4/11/2022 4/25/2022 14 14 OK MW-31 Thallium 4/11/2022 4/26/2022 15 180 OK MW-31 Tin 4/11/2022 4/27/2022 16 180 OK MW-31 Toluene 4/11/2022 4/25/2022 14 14 OK MW-31 Total Dissolved Solids 4/11/2022 4/18/2022 7 7 OK MW-31 Uranium 4/11/2022 4/26/2022 15 180 OK MW-31 Vanadium 4/11/2022 4/26/2022 15 180 OK MW-31 X ylenes, total 4/11/2022 4/25/2022 14 14 OK MW-31 Zinc 4/11/2022 4/26/2022 15 180 OK MW-32 Acetone 4/11/2022 4/25/2022 14 14 OK MW-32 Arsenic 4/11/2022 4/26/2022 15 180 OK MW-32 Benzene 4/11/2022 4/25/2022 14 14 OK MW-32 Beryllium 4/11/2022 4/26/2022 15 180 OK MW-32 Bicarbonate as CaC03 4/11/2022 4/16/2022 5 14 OK MW-32 Cadmium 4/11/2022 4/26/2022 15 180 OK MW-32 Calcium 4/11/2022 4/26/2022 15 180 OK MW-32 Carbon Tetrachloride 4/11/2022 4/25/2022 14 14 OK MW-32 Carbonate as C03 4/11/2022 4/16/2022 5 14 OK MW-32 Chloride 4/11/2022 4/18/2022 7 28 OK MW-32 Chloroform 4/11/2022 4/25/2022 14 14 OK MW-32 Chloromethane 4/11/2022 4/25/2022 14 14 OK MW-32 Chromium 4/11/2022 4/26/2022 15 180 OK MW-32 Cobalt 4/11/2022 4/26/2022 15 180 OK MW-32 Copper 4/11/2022 4/26/2022 15 180 OK MW-32 Fluoride 4/11/2022 4/18/2022 7 28 OK MW-32 Gross Radium Alpha 4/11/2022 5/10/2022 29 180 OK MW-32 Iron 4/11/2022 4/26/2022 15 180 OK MW-32 Lead 4/11/2022 4/26/2022 15 180 OK MW-32 Magnesium 4/11/2022 4/26/2022 15 180 OK MW-32 Manganese 4/11/2022 4/26/2022 15 180 OK MW-32 Mercury 4/11/2022 4/26/2022 15 180 OK MW-32 Methyl Ethyl Ketone 4/11/2022 4/25/2022 14 14 OK MW-32 Methylene Chloride 4/11/2022 4/25/2022 14 14 OK MW-32 Molybdenum 4/11/2022 4/26/2022 15 180 OK MW-32 NaphLhalene 4/11/2022 4/25/2022 14 14 OK MW-32 Nickel 4/11/2022 4/26/2022 15 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-32 Nitrate + Nitrite as N 4/11/2022 4/21/2022 10 28 OK MW-32 Nitrogen, Ammonia as N 4/11/2022 4/25/2022 14 28 OK MW-32 Potassium 4/11/2022 4/26/2022 15 180 OK MW-32 Selenium 4/11/2022 4/26/2022 15 180 OK MW-32 Silver 4/11/2022 4/26/2022 15 180 OK MW-32 Sodium 4/11/2022 4/26/2022 15 180 OK MW-32 Sulfate 4/11/2022 4/19/2022 8 28 OK MW-32 Tetrahydrofuran 4/11/2022 4/25/2022 14 14 OK MW-32 Thallium 4/11/2022 4/26/2022 15 180 OK MW-32 Tin 4/11/2022 5/16/2022 35 180 OK MW-32 Toluene 4/11/2022 4/25/2022 14 14 OK MW-32 Uranium 4/11/2022 4/26/2022 15 180 OK MW-32 Vanadium 4/11/2022 4/26/2022 15 180 OK MW-32 Xylenes, total 4/11/2022 4/25/2022 14 14 OK MW-32 Zinc 4/11/2022 4/26/2022 15 180 OK MW-32 Total Dissolved Solids 5/16/2022 5/19/2022 3 7 OK MW-35 Acetone 4/12/2022 4/25/2022 13 14 OK MW-35 Arsenic 4/12/2022 4/26/2022 14 180 OK MW-35 Benzene 4/12/2022 4/25/2022 13 14 OK MW-35 Beryllium 4/12/2022 4/26/2022 14 180 OK MW-35 Bicarbonate as CaC03 4/12/2022 4/16/2022 4 14 OK MW-35 Cadmium 4/12/2022 4/26/2022 14 180 OK MW-35 Calcium 4/12/2022 4/27/2022 15 180 OK MW-35 Carbon Tetrachloride 4/12/2022 4/25/2022 13 14 OK MW-35 Carbonate as C03 4/12/2022 4/16/2022 4 14 OK MW-35 Chloride 4/12/2022 4/19/2022 7 28 OK MW-35 Chloroform 4/12/2022 4/25/2022 13 14 OK MW-35 Chloromethane 4/12/2022 4/25/2022 13 14 OK MW-35 Chromium 4/12/2022 4/26/2022 14 180 OK MW-35 Cobalt 4/12/2022 4/26/2022 14 180 OK MW-35 Copper 4/12/2022 4/26/2022 14 180 OK MW-35 Fluoride 4/12/2022 5/4/2022 22 28 OK MW-35 Gross Radium Aloha 4/12/2022 5/10/2022 28 180 OK MW-35 Iron 4/12/2022 4/27/2022 15 180 OK MW-35 Lead 4/12/2022 4/26/2022 14 180 OK MW-35 Magnesium 4/12/2022 4/27/2022 15 180 OK MW-35 Manganese 4/12/2022 4/26/2022 14 180 OK MW-35 Mercury 4/12/2022 4/26/2022 14 180 OK MW-35 Methyl Ethyl Ketone 4/12/2022 4/25/2022 13 14 OK MW-35 Methylene Chloride 4/12/2022 4/25/2022 13 14 OK MW-35 Molybdenum 4/12/2022 4/26/2022 14 180 OK MW-35 Naphthalene 4/12/2022 4/25/2022 13 14 OK MW-35 Nickel 4/12/2022 4/26/2022 14 180 OK MW-35 Nitrate + Nitrite as N 4/12/2022 4/21/2022 9 28 OK MW-35 Nitrogen, Ammonia as N 4/12/2022 4/25/2022 13 28 OK MW-35 Potassium 4/12/2022 4/27/2022 15 180 OK MW-35 Selenium 4/12/2022 4/26/2022 14 180 OK MW-35 Silver 4/12/2022 4/26/2022 14 180 OK MW-35 Sodium 4/12/2022 4/27/2022 15 180 OK MW-35 Sulfate 4/12/2022 4/19/2022 7 28 OK MW-35 Tetrahydrofuran 4/12/2022 4/25/2022 13 14 OK MW-35 Thallium 4/12/2022 4/26/2022 14 180 OK MW-35 Tin 4/12/2022 4/27/2022 15 180 OK G-2A: Quarterly Holding Time Evaluation l Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-35 Toluene 4/12/2022 4/25/2022 13 14 OK MW-35 Total Dissolved Solids 4/12/2022 4/18/2022 6 7 OK MW-35 Uranium 4/12/2022 4/26/2022 14 180 OK MW-35 Vanadium 4/12/2022 4/26/2022 14 180 OK MW-35 Xylenes, total 4/12/2022 4/25/2022 13 14 OK MW-35 Zinc 4/12/2022 4/26/2022 14 180 OK MW-36 Acetone 4/21/2022 4/26/2022 5 14 OK MW-36 Arsenic 4/21/2022 5/2/2022 11 180 OK MW-36 Benzene 4/21/2022 4/26/2022 5 14 OK MW-36 Beryllium 4/21/2022 5/2/2022 11 180 OK MW-36 Bicarbonate as CaC03 4/21/2022 4/23/2022 2 14 OK MW-36 Cadmium 4/21/2022 5/2/2022 11 180 OK MW-36 Calcium 4/21/2022 5/2/2022 11 180 OK MW-36 Carbon Tetrachloride 4/21/2022 4/26/2022 5 14 OK MW-36 Carbonate as C03 4/21/2022 4/23/2022 2 14 OK MW-36 Chloride 4/21/2022 5/3/2022 12 28 OK MW-36 Chloroform 4/21/2022 4/26/2022 5 14 OK MW-36 Chloromethane 4/21/2022 4/26/2022 5 14 OK MW-36 Chromium 4/21/2022 5/2/2022 11 180 OK MW-36 Cobalt 4/21/2022 5/2/2022 11 180 OK MW-36 Cooper 4/21/2022 5/2/2022 11 180 OK MW-36 Fluoride 4/21/2022 5/19/2022 28 28 OK MW-36 Gross Radium Aloha 4/21/2022 5/18/2022 27 180 OK MW-36 Iron 4/21/2022 5/2/2022 11 180 OK MW-36 Lead 4/21/2022 5/2/2022 11 180 OK MW-36 Magnesium 4/21/2022 5/2/2022 11 180 OK MW-36 Manganese 4/21/2022 5/2/2022 11 180 OK MW-36 Mercury 4/21/2022 5/3/2022 12 180 OK MW-36 Methyl Ethyl Ketone 4/21/2022 4/26/2022 5 14 OK MW-36 Methylene Chloride 4/21/2022 4/26/2022 5 14 OK MW-36 Molybdenum 4/21/2022 5/2/2022 11 180 OK MW-36 Naphthalene 4/21/2022 4/26/2022 5 14 OK MW-36 Nickel 4/21/2022 5/2/2022 11 180 OK MW-36 Nitrate + Nitrite as N 4/21/2022 4/25/2022 4 28 OK MW-36 Nitrogen, Ammonia as N 4/21/2022 5/5/2022 14 28 OK MW-36 Potassium 4/21/2022 5/2/2022 11 180 OK MW-36 Selenium 4/21/2022 5/2/2022 11 180 OK MW-36 Silver 4/21/2022 5/2/2022 11 180 OK MW-36 Sodium 4/21/2022 5/2/2022 11 180 OK MW-36 Sulfate 4/21/2022 4/27/2022 6 28 OK MW-36 Tetrahydrofuran 4/21/2022 4/26/2022 5 14 OK MW-36 Thallium 4/21/2022 5/2/2022 11 180 OK MW-36 Tin 4/21/2022 5/2/2022 11 180 OK MW-36 Toluene 4/21/2022 4/26/2022 5 14 OK MW-36 Total Dissolved Solids 4/21/2022 4/25/2022 4 7 OK MW-36 Uranium 4/21/2022 5/2/2022 11 180 OK MW-36 Vanadium 4/21/2022 5/2/2022 11 180 OK MW-36 Xylenes, total 4/21/2022 4/26/2022 5 14 OK MW-36 Zinc 4/21/2022 5/2/2022 11 180 OK MW-37 Acetone 5/17/2022 5/25/2022 8 14 OK MW-37 Arsenic 5/17/2022 5/27/2022 10 180 OK MW-37 Benzene 5/17/2022 5/25/2022 8 14 OK MW-37 Beryllium 5/17/2022 5/27/2022 10 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-37 Bicarbonate as CaC03 5/17/2022 5/24/2022 7 14 OK MW-37 Cadmium 5/17/2022 5/27/2022 10 180 OK MW-37 Calcium 5/17/2022 5/27/2022 IO 180 OK MW-37 Carbon Tetrachloride 5/17/2022 5/25/2022 8 14 OK MW-37 Carbonate as C03 5/17/2022 5/24/2022 7 14 OK MW-37 Chloride 5/17/2022 5/25/2022 8 28 OK MW-37 Chloroform 5/17/2022 5/25/2022 8 14 OK MW-37 Chloromethane 5/17/2022 5/25/2022 8 14 OK MW-37 Chromium 5/17/2022 5/27/2022 10 180 OK MW-37 Cobalt 5/17/2022 5/27/2022 IO 180 OK MW-37 Copper 5/17/2022 5/27/2022 10 180 OK MW-37 Fluoride 5/17/2022 5/25/2022 8 28 OK MW-37 Gross Radium Alpha 5/17/2022 5/24/2022 7 180 OK MW-37 Iron 5/17/2022 5/27/2022 IO 180 OK MW-37 Lead 5/17/2022 5/27/2022 IO 180 OK MW-37 Magnesium 5/17/2022 5/27/2022 IO 180 OK MW-37 Manganese 5/17/2022 5/27/2022 10 180 OK MW-37 Mercury 5/17/2022 5/20/2022 3 180 OK MW-37 Methyl Ethyl Ketone 5/17/2022 5/25/2022 8 14 OK MW-37 Methylene Chloride 5/17/2022 5/25/2022 8 14 OK MW-37 Molybdenum 5/17/2022 5/27/2022 IO 180 OK MW-37 Naphthalene 5/17/2022 5/25/2022 8 14 OK MW-37 Nickel 5/17/2022 5/27/2022 IO 180 OK MW-37 Nitrate + Nitrite as N 5/17/2022 5/24/2022 7 28 OK MW-37 Nitrogen, Ammonia as N 5/17/2022 5/27/2022 10 28 OK MW-37 Potassium 5/17/2022 5/27/2022 IO 180 OK MW-37 Selenium 5/17/2022 5/27/2022 10 180 OK MW-37 Silver 5/17/2022 5/27/2022 IO 180 OK MW-37 Sodium 5/17/2022 5/27/2022 10 180 OK MW-37 Sulfate 5/17/2022 5/31/2022 14 28 OK MW-37 Tetrahydrofuran 5/17/2022 5/25/2022 8 14 OK MW-37 Thallium 5/17/2022 5/27/2022 IO 180 OK MW-37 Tin 5/17/2022 5/27/2022 IO 180 OK MW-37 Toluene 5/17/2022 5/25/2022 8 14 OK MW-37 Total Dissolved Solids 5/17/2022 5/19/2022 2 7 OK MW-37 Uranium 5/17/2022 5/27/2022 IO 180 OK MW-37 Vanadium 5/17/2022 5/27/2022 10 180 OK MW-37 Xylenes, total 5/17/2022 5/25/2022 8 14 OK MW-37 Zinc 5/17/2022 5/27/2022 10 180 OK MW-38 Acetone 4/27/2022 5/3/2022 6 14 OK MW-38 Arsenic 4/27/2022 5/10/2022 13 180 OK MW-38 Benzene 4/27/2022 5/3/2022 6 14 OK MW-38 Beryllium 4/27/2022 5/10/2022 13 180 OK MW-38 Bicarbonate as CaC03 4/27/2022 5/3/2022 6 14 OK MW-38 Cadmium 4/27/2022 5/10/2022 13 180 OK MW-38 Calcium 4/27/2022 5/10/2022 13 180 OK MW-38 Carbon Tetrachloride 4/27/2022 5/3/2022 6 14 OK MW-38 Carbonate as C03 4/27/2022 5/3/2022 6 14 OK MW-38 Chloride 4/27/2022 5/8/2022 11 28 OK MW-38 Chloroform 4/27/2022 5/3/2022 6 14 OK MW-38 Chloromethane 4/27/2022 5/3/2022 6 14 OK MW-38 Chromium 4/27/2022 5/10/2022 13 180 OK MW-38 Cobalt 4/27/2022 5/10/2022 13 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-38 Copper 4/27/2022 5/10/2022 13 180 OK MW-38 Fluoride 4/27/2022 5/4/2022 7 28 OK MW-38 Gross Radium Alpha 4/27/2022 5/24/2022 27 180 OK MW-38 Iron 4/27/2022 5/10/2022 13 180 OK MW-38 Lead 4/27/2022 5/10/2022 13 180 OK MW-38 Magnesium 4/27/2022 5/10/2022 13 180 OK MW-38 Manganese 4/27/2022 5/10/2022 13 180 OK MW-38 Mercury 4/27/2022 5/4/2022 7 180 OK MW-38 Methyl Ethyl Ketone 4/27/2022 5/3/2022 6 14 OK MW-38 Methylene Chloride 4/27/2022 5/3/2022 6 14 OK MW-38 Molybdenum 4/27/2022 5/10/2022 13 180 OK MW-38 Naphthalene 4/27/2022 5/3/2022 6 14 OK MW-38 Nickel 4/27/2022 5/10/2022 13 180 OK MW-38 Nitrate + Nitrite as N 4/27/2022 4/30/2022 3 28 OK MW-38 Nitrogen, Ammonia as N 4/27/2022 5/12/2022 15 28 OK MW-38 Potassium 4/27/2022 5/10/2022 13 180 OK MW-38 Selenium 4/27/2022 5/10/2022 13 180 OK MW-38 Silver 4/27/2022 5/10/2022 13 180 OK MW-38 Sodium 4/27/2022 5/11/2022 14 180 OK MW-38 Sulfate 4/27/2022 5/8/2022 11 28 OK MW-38 Tetrahydrofuran 4/27/2022 5/3/2022 6 14 OK MW-38 Thallium 4/27/2022 5/10/2022 13 180 OK MW-38 Tin 4/27/2022 5/10/2022 13 180 OK MW-38 Toluene 4/27/2022 5/3/2022 6 14 OK MW-38 Total Dissolved Solids 4/27/2022 5/2/2022 5 7 OK MW-38 Uranium 4/27/2022 5/10/2022 13 180 OK MW-38 Vanadium 4/27/2022 5/10/2022 13 180 OK MW-38 Xylenes, total 4/27/2022 5/3/2022 6 14 OK MW-38 Zinc 4/27/2022 5/10/2022 13 180 OK MW-39 Acetone 4/20/2022 4/26/2022 6 14 OK MW-39 Arsenic 4/20/2022 5/2/2022 12 180 OK MW-39 Benzene 4/20/2022 4/26/2022 6 14 OK MW-39 Beryllium 4/20/2022 5/2/2022 12 180 OK MW-39 Bicarbonate as CaC03 4/20/2022 4/24/2022 4 14 OK MW-39 Cadmium 4/20/2022 5/2/2022 12 180 OK MW-39 Calcium 4/20/2022 5/2/2022 12 180 OK MW-39 Carbon Tetrachloride 4/20/2022 4/26/2022 6 14 OK MW-39 Carbonate as C03 4/20/2022 4/24/2022 4 14 OK MW-39 Chloride 4/20/2022 5/3/2022 13 28 OK MW-39 Chloroform 4/20/2022 4/26/2022 6 14 OK MW-39 Chloromethane 4/20/2022 4/26/2022 6 14 OK MW-39 Chromium 4/20/2022 5/2/2022 12 180 OK MW-39 Cobalt 4/20/2022 5/2/2022 12 180 OK MW-39 Copper 4/20/2022 5/2/2022 12 180 OK MW-39 Fluoride 4/20/2022 5/3/2022 13 28 OK MW-39 Gross Radium Alpha 4/20/2022 5/18/2022 28 180 OK MW-39 Iron 4/20/2022 5/2/2022 12 180 OK MW-39 Lead 4/20/2022 5/2/2022 12 180 OK MW-39 Magnesium 4/20/2022 5/2/2022 12 180 OK MW-39 Manganese 4/20/2022 5/2/2022 12 180 OK MW-39 Mercury 4/20/2022 5/3/2022 13 180 OK MW-39 Methyl Ethyl Ketone 4/20/2022 4/26/2022 6 14 OK MW-39 Methylene Chloride 4/20/2022 4/26/2022 6 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name SamP.le Date Analysis Date (Days) Time (Days) Check MW-39 Molybdenum 4/20/2022 5/2/2022 12 180 OK MW-39 Naphthalene 4/20/2022 4/26/2022 6 14 OK MW-39 Nickel 4/20/2022 5/2/2022 12 180 OK MW-39 Nitrate + Nitrite as N 4/20/2022 4/25/2022 5 28 OK MW-39 Nitrogen, Ammonia as N 4/20/2022 5/5/2022 15 28 OK MW-39 Potassium 4/20/2022 5/2/2022 12 180 OK MW-39 Selenium 4/20/2022 5/2/2022 12 180 OK MW-39 Silver 4/20/2022 5/2/2022 12 180 OK MW-39 Sodium 4/20/2022 5/2/2022 12 180 OK MW-39 Sulfate 4/20/2022 4/27/2022 7 28 OK MW-39 Tetrahydrofuran 4/20/2022 4/26/2022 6 14 OK MW-39 Thallium 4/20/2022 5/2/2022 12 180 OK MW-39 Tin 4/20/2022 5/2/2022 12 180 OK MW-39 Toluene 4/20/2022 4/26/2022 6 14 OK MW-39 Total Dissolved Solids 4/20/2022 4/25/2022 5 7 OK MW-39 Uranium 4/20/2022 5/2/2022 12 180 OK MW-39 Vanadium 4/20/2022 5/2/2022 12 180 OK MW-39 Xylenes, total 4/20/2022 4/26/2022 6 14 OK MW-39 Zinc 4/20/2022 5/2/2022 12 180 OK MW-40 Acetone 4/19/2022 4/27/2022 8 14 OK MW-40 Arsenic 4/19/2022 5/2/2022 13 180 OK MW-40 Benzene 4/19/2022 4/27/2022 8 14 OK MW-40 Beryllium 4/19/2022 5/2/2022 13 180 OK MW-40 Bicarbonate as CaC03 4/19/2022 4/23/2022 4 14 OK MW-40 Cadmium 4/19/2022 5/2/2022 13 180 OK MW-40 Calcium 4/19/2022 5/2/2022 13 180 OK MW-40 Carbon Tetrachloride 4/19/2022 4/27/2022 8 14 OK MW-40 Carbonate as C03 4/19/2022 4/23/2022 4 14 OK MW-40 Chloride 4/19/2022 5/2/2022 13 28 OK MW-40 Chloroform 4/19/2022 4/27/2022 8 14 OK MW-40 Chloromethane 4/19/2022 4/27/2022 8 14 OK MW-40 Chromium 4/19/2022 5/2/2022 13 180 OK MW-40 Cobalt 4/19/2022 5/2/2022 13 180 OK MW-40 Coooer 4/19/2022 5/2/2022 13 180 OK MW-40 Fluoride 4/19/2022 5/2/2022 13 28 OK MW-40 Gross Radium Alpha 4/19/2022 5/18/2022 29 180 OK MW-40 Iron 4/19/2022 5/2/2022 13 180 OK MW-40 Lead 4/19/2022 5/2/2022 13 180 OK MW-40 Magnesium 4/19/2022 5/2/2022 13 180 OK MW-40 Manganese 4/19/2022 5/2/2022 13 180 OK MW-40 Mercury 4/19/2022 5/3/2022 14 180 OK MW-40 Methyl Ethyl Ketone 4/19/2022 4/27/2022 8 14 OK MW-40 Methylene Chloride 4/19/2022 4/27/2022 8 14 OK MW-40 Molybdenum 4/19/2022 5/2/2022 13 180 OK MW-40 Naphthalene 4/19/2022 4/27/2022 8 14 OK MW-40 Nickel 4/19/2022 5/2/2022 13 180 OK MW-40 Nitrate + Nitrite as N 4/19/2022 4/25/2022 6 28 OK MW-40 Nitrogen, Ammonia as N 4/19/2022 5/5/2022 16 28 OK MW-40 Potassium 4/19/2022 5/2/2022 13 180 OK MW-40 Selenium 4/19/2022 5/2/2022 13 180 OK MW-40 Silver 4/19/2022 5/2/2022 13 180 OK MW-40 Sodium 4/19/2022 5/2/2022 13 180 OK MW-40 Sulfate 4/19/2022 4/27/2022 8 28 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-40 Tetrahydrofuran 4/19/2022 4/27/2022 8 14 OK MW-40 Thallium 4/19/2022 5/2/2022 13 180 OK MW-40 Tin 4/19/2022 5/2/2022 13 180 OK MW-40 Toluene 4/19/2022 4/27/2022 8 14 OK MW-40 Total Dissolved Solids 4/19/2022 4/25/2022 6 7 OK MW-40 Uranium 4/19/2022 5/2/2022 13 180 OK MW-40 Vanadium 4/19/2022 5/2/2022 13 180 OK MW-40 Xylenes, total 4/19/2022 4/27/2022 8 14 OK MW-40 Zinc 4/19/2022 5/2/2022 13 180 OK MW-65 Acetone 4/14/2022 4/26/2022 12 14 OK MW-65 Arsenic 4/14/2022 4/26/2022 12 180 OK MW-65 Benzene 4/14/2022 4/26/2022 12 14 OK MW-65 Beryllium 4/14/2022 4/26/2022 12 180 OK MW-65 Bicarbonate as CaC03 4/14/2022 4/16/2022 2 14 OK MW-65 Cadmium 4/14/2022 4/26/2022 12 180 OK MW-65 Calcium 4/14/2022 4/27/2022 13 180 OK MW-65 Carbon Tetrachloride 4/14/2022 4/26/2022 12 14 OK MW-65 Carbonate as C03 4/14/2022 4/16/2022 2 14 OK MW-65 Chloride 4/14/2022 4/19/2022 5 28 OK MW-65 Chloroform 4/14/2022 4/26/2022 12 14 OK MW-65 Chloromethane 4/14/2022 4/26/2022 12 14 OK MW-65 Chromium 4/14/2022 4/26/2022 12 180 OK MW-65 Cobalt 4/14/2022 4/26/2022 12 180 OK MW-65 Copper 4/14/2022 4/26/2022 12 180 OK MW-65 Fluoride 4/14/2022 4/19/2022 5 28 OK MW-65 Gross Radium Alpha 4/14/2022 5/10/2022 26 180 OK MW-65 Iron 4/14/2022 4/27/2022 13 180 OK MW-65 Lead 4/14/2022 4/26/2022 12 180 OK MW-65 Magnesium 4/14/2022 4/27/2022 13 180 OK MW-65 Manganese 4/14/2022 4/26/2022 12 180 OK MW-65 Mercury 4/14/2022 4/26/2022 12 180 OK MW-65 Methyl Ethyl Ketone 4/14/2022 4/26/2022 12 14 OK MW-65 Methylene Chloride 4/14/2022 4/26/2022 12 14 OK MW-65 Molybdenum 4/14/2022 4/26/2022 12 180 OK MW-65 Naphthalene 4/14/2022 4/26/2022 12 14 OK MW-65 Nickel 4/14/2022 4/26/2022 12 180 OK MW-65 Nitrate+ Nitrite as N 4/14/2022 4/21/2022 7 28 OK MW-65 Nitrogen, Ammonia as N 4/14/2022 4/25/2022 11 28 OK MW-65 Potassium 4/14/2022 4/27/2022 13 180 OK MW-65 Selenium 4/14/2022 4/26/2022 12 180 OK MW-65 Silver 4/14/2022 4/26/2022 12 180 OK MW-65 Sodium 4/14/2022 4/27/2022 13 180 OK MW-65 Sulfate 4/14/2022 4/19/2022 5 28 OK MW-65 Tetrahydrofuran 4/14/2022 4/26/2022 12 14 OK MW-65 Thallium 4/14/2022 4/26/2022 12 180 OK MW-65 Tin 4/14/2022 4/27/2022 13 180 OK MW-65 Toluene 4/14/2022 4/26/2022 12 14 OK MW-65 Total Dissolved Solids 4/14/2022 4/19/2022 5 7 OK MW-65 Uranium 4/14/2022 4/26/2022 12 180 OK MW-65 Vanadium 4/14/2022 4/26/2022 12 180 OK MW-65 Xylenes, total 4/14/2022 4/26/2022 12 14 OK MW-65 Zinc 4/14/2022 4/26/2022 12 180 OK MW-70 Acetone 4/21/2022 4/26/2022 5 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-70 Arsenic 4/21/2022 5/2/2022 11 180 OK MW-70 Benzene 4/21/2022 4/26/2022 5 14 OK MW-70 :SeryHium 4/21/2022 5/2/2022 11 180 OK MW-70 Bicarbonate as CaC03 4/21/2022 4/23/2022 2 14 OK MW-70 Cadmium 4/21/2022 5/2/2022 11 180 OK MW-70 Calcium 4/21/2022 5/2/2022 11 180 OK MW-70 Carbon Tetrachloride 4/21/2022 4/26/2022 5 14 OK MW-70 Carbonate as C03 4/21/2022 4/23/2022 2 14 OK MW-70 Chloride 4/21/2022 5/3/2022 12 28 OK MW-70 Chloroform 4/21/2022 4/26/2022 5 14 OK MW-70 Chloromethane 4/21/2022 4/26/2022 5 14 OK MW-70 Chromium 4/21/2022 5/2/2022 11 180 OK MW-70 Cobalt 4/21/2022 5/2/2022 11 180 OK MW-70 Copper 4/21/2022 5/2/2022 11 180 OK MW-70 Fluoride 4/21/2022 5/19/2022 28 28 OK MW-70 Gross Radium Alpha 4/21/2022 5/18/2022 27 180 OK MW-70 Iron 4/21/2022 5/2/2022 11 180 OK MW-70 Lead 4/21/2022 5/2/2022 11 180 OK MW-70 Magnesium 4/21/2022 5/2/2022 11 180 OK MW-70 Manj!;anese 4/21/2022 5/2/2022 11 180 OK MW-70 Mercury 4/21/2022 5/3/2022 12 180 OK MW-70 Methyl Ethyl Ketone 4/21/2022 4/26/2022 5 14 OK MW-70 Methylene Chloride 4/21/2022 4/26/2022 5 14 OK MW-70 Molybdenum 4/21/2022 5/2/2022 11 180 OK MW-70 Naphthalene 4/21/2022 4/26/2022 5 14 OK MW-70 Nickel 4/21/2022 5/2/2022 11 180 OK MW-70 Nitrate + Nitrite as N 4/21/2022 4/25/2022 4 28 OK MW-70 Nitrogen, Ammonia as N 4/21/2022 5/5/2022 14 28 OK MW-70 Potassium 4/21/2022 5/2/2022 11 180 OK MW-70 Selenium 4/21/2022 5/2/2022 11 180 OK MW-70 Silver 4/21/2022 5/2/2022 11 180 OK MW-70 Sodium 4/21/2022 5/2/2022 11 180 OK MW-70 Sulfate 4/21/2022 4/27/2022 6 28 OK MW-70 Tctrahvdrofuran 4/21/2022 4/26/2022 5 14 OK MW-70 Thallium 4/21/2022 5/2/2022 11 180 OK MW-70 Tin 4/21/2022 5/2/2022 11 180 OK MW-70 Toluene 4/21/2022 4/26/2022 5 14 OK MW-70 Total Dissolved Solids 4/21/2022 4/25/2022 4 7 OK MW-70 Uranium 4/21/2022 5/2/2022 11 180 OK MW-70 Vanadium 4/21/2022 5/2/2022 11 180 OK MW-70 Xylenes, total 4/21/2022 4/26/2022 5 14 OK MW-70 Zinc 4/21/2022 5/2/2022 11 180 OK TW4-24 Acetone 4/27/2022 5/3/2022 6 14 OK TW4-24 Arsenic 4/27/2022 5/5/2022 8 180 OK TW4-24 Benzene 4/27/2022 5/3/2022 6 14 OK TW4-24 Beryllium 4/27/2022 5/5/2022 8 180 OK TW4-24 Bicarbonate as CaC03 4/27/2022 5/4/2022 7 14 OK TW4-24 Cadmium 4/27/2022 5/5/2022 8 180 OK TW4-24 Calcium 4/27/2022 5/10/2022 13 180 OK TW4-24 Carbon Tetrachloride 4/27/2022 5/3/2022 6 14 OK TW4-24 Carbonate as C03 4/27/2022 5/4/2022 7 14 OK TW4-24 Chloride 4/27/2022 5/8/2022 11 28 OK TW4-24 Chloroform 4/27/2022 5/3/2022 6 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check TW4-24 Chloromethane 4/27/2022 5/3/2022 6 14 OK TW4-24 Chromium 4/27/2022 5/5/2022 8 180 OK TW4-24 Cobalt 4/27/2022 5/5/2022 8 180 OK TW4-24 Copper 4/27/2022 5/5/2022 8 180 OK TW4-24 Fluoride 4/27/2022 5/4/2022 7 28 OK TW4-24 Gross Radium Alpha 4/27/2022 5/24/2022 27 180 OK TW4-24 Iron 4/27/2022 5/11/2022 14 180 OK TW4-24 Lead 4/27/2022 5/5/2022 8 180 OK TW4-24 Magnesium 4/27/2022 5/10/2022 13 180 OK TW4-24 Manganese 4/27/2022 5/5/2022 8 180 OK TW4-24 Mercury 4/27/2022 5/4/2022 7 180 OK TW4-24 Methyl Ethyl Ketone 4/27/2022 5/3/2022 6 14 OK TW4-24 Methylene Chloride 4/27/2022 5/3/2022 6 14 OK TW4-24 Molybdenum 4/27/2022 5/5/2022 8 180 OK TW4-24 Naphthalene 4/27/2022 5/3/2022 6 14 OK TW4-24 Nickel 4/27/2022 5/5/2022 8 180 OK TW4-24 Nitrate + Nitrite as N 4/27/2022 4/30/2022 3 28 OK TW4-24 Nitrogen, Ammonia as N 4/27/2022 5/12/2022 15 28 OK TW4-24 Potassium 4/27/2022 5/10/2022 13 180 OK TW4-24 Selenium 4/27/2022 5/5/2022 8 180 OK TW4-24 Silver 4/27/2022 5/5/2022 8 180 OK TW4-24 Sodium 4/27/2022 5/11/2022 14 180 OK TW4-24 Sulfate 4/27/2022 5/8/2022 11 28 OK TW4-24 Tetrahydrofuran 4/27/2022 5/3/2022 6 14 OK TW4-24 Thallium 4/27/2022 5/5/2022 8 180 OK TW4-24 Tin 4/27/2022 5/10/2022 13 180 OK TW4-24 Toluene 4/27/2022 5/3/2022 6 14 OK TW4-24 Total Dissolved Solids 4/27/2022 5/2/2022 5 7 OK TW4-24 Uranium 4/27/2022 5/5/2022 8 180 OK TW4-24 Vanadium 4/27/2022 5/5/2022 8 180 OK TW4-24 Xylenes, total 4/27/2022 5/3/2022 6 14 OK TW4-24 Zinc 4/27/2022 5/5/2022 8 180 OK G-2B: Accelerated Holding Time Evaluation I Allowed Hold Time Hold Time Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) (Days) Check Trip Blank Chloroform 5/4/2022 5/11/2022 7 14 OK Trip Blank Toluene 6/7/2022 6/17/2022 10 14 OK Trip Blank Tetrahydrnfuran 6/7/2022 6/17/2022 10 14 OK Trip Blank Xvlenes, total 6/7/2022 6/17/2022 10 14 OK Trip Blank Carbon Tetrachloride 6/7/2022 6/17/2022 10 14 OK Trip Blank Acetone 6/7/2022 6/17/2022 10 14 OK Trip Blank Chloroform 6/7/2022 6/17/2022 10 14 OK Trip Blank Benzene 6/7/2022 6/17/2022 10 14 OK Trip Blank Chloromethane 6/7/2022 6/17/2022 10 14 OK Trip Blank Methylene Chloride 6/7/2022 6/17/2022 10 14 OK Trip Blank Methyl Ethyl Ketone 6/7/2022 6/17/2022 10 14 OK Trip Blank Naphthalene 6/7/2022 6/17/2022 10 14 OK MW-11 Sulfate 5/4/2022 5/19/2022 15 28 OK MW-11 Chloride 5/4/2022 5/11/2022 7 28 OK MW-11 Manganese 5/4/2022 5/16/2022 12 180 OK MW-11 Nitrate + Nitrite as N 5/4/2022 5/9/2022 5 28 OK MW-11 Total Dissolved Solids 5/4/2022 5/9/2022 5 7 OK MW-11 Sulfate 6/6/2022 6/15/2022 9 28 OK MW-11 Chloride 6/6/2022 6/15/2022 9 28 OK MW-11 Manganese 6/6/2022 6/15/2022 9 180 OK MW-11 Nitrate + Nitrite as N 6/6/2022 6/20/2022 14 28 OK MW-11 Total Dissolved Solids 6/6/2022 6/10/2022 4 7 OK MW-25 Total Dissolved Solids 5/3/2022 5/9/2022 6 7 OK MW-25 Total Dissolved Solids 6/7/2022 6/10/2022 3 7 OK MW-26 Chloride 5/4/2022 5/11/2022 7 28 OK MW-26 Chloroform 5/4/2022 5/13/2022 9 14 OK MW-26 Nitrate + Nitrite as N 5/4/2022 5/9/2022 5 28 OK MW-26 Total Dissolved Solids 5/4/2022 5/10/2022 6 7 OK MW-26 Toluene 6/7/2022 6/17/2022 10 14 OK MW-26 Tetrahydrof uran 6/7/2022 6/17/2022 10 14 OK MW-26 Xylenes, total 6/7/2022 6/17/2022 10 14 OK MW-26 Chloride 6/7/2022 6/15/2022 8 28 OK MW-26 Carbon Tetrachloride 6/7/2022 6/17/2022 10 14 OK MW-26 Acetone 6/7/2022 6/17/2022 10 14 OK MW-26 Chloroform 6/7/2022 6/17/2022 10 14 OK MW-26 Benzene 6/7/2022 6/17/2022 10 14 OK MW-26 Chloromethane 6/7/2022 6/17/2022 10 14 OK MW-26 Methylene Chloride 6/7/2022 6/17/2022 10 14 OK MW-26 Methyl Ethyl Ketone 6/7/2022 6/17/2022 10 14 OK MW-26 Naphthalene 6/7/2022 6/17/2022 10 14 OK MW-26 Nitrate + Nitrite as N 6/7/2022 6/20/2022 13 28 OK MW-26 Total Dissolved Solids 6/7/2022 6/10/2022 3 7 OK MW-30 Chloride 5/4/2022 5/11/2022 7 28 OK MW-30 Uranium 5/4/2022 5/16/2022 12 180 OK MW-30 Selenium 5/4/2022 5/16/2022 12 180 OK MW-30 Nitrate+ Nitrite as N 5/4/2022 5/9/2022 5 28 OK MW-30 Total Dissolved Solids 5/4/2022 5/9/2022 5 7 OK MW-30 Chloride 6/7/2022 6/15/2022 8 28 OK MW-30 Uranium 6/7/2022 6/15/2022 8 180 OK MW-30 Selenium 6/7/2022 6/15/2022 8 180 OK MW-30 Nitrate + Nitrite as N 6/7/2022 6/13/2022 6 28 OK MW-30 Total Dissolved Solids 6/7/2022 6/10/2022 3 7 OK MW-31 Sulfate 5/3/2022 5/12/2022 9 28 OK G-2B: Accelerated Holding Time Evaluation Allowed Hold Time Hold Time Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) (Days) Check MW-31 Chloride 5/3/2022 5/12/2022 9 28 OK MW-31 Uranium 5/3/2022 5/16/2022 13 180 OK MW-31 Nitrate + Nitrite as N 5/3/2022 5/9/2022 6 28 OK MW-31 Total Dissolved Solids 5/3/2022 5/9/2022 6 7 OK MW-31 Sulfate 6/6/2022 6/21/2022 15 28 OK MW-31 Chloride 6/6/2022 6/16/2022 10 28 OK MW-31 Uranium 6/6/2022 6/15/2022 9 180 OK MW-31 Nitrate+ Nitrite as N 6/6/2022 6/13/2022 7 28 OK MW-31 Total Dissolved Solids 6/6/2022 6/10/2022 4 7 OK MW-65 Chloride 5/4/2022 5/12/2022 8 28 OK MW-65 Uranium 5/4/2022 5/16/2022 12 180 OK MW-65 Selenium 5/4/2022 5/16/2022 12 180 OK MW-65 Nitrate + Nitrite as N 5/4/2022 5/9/2022 5 28 OK MW-65 Total Dissolved Solids 5/4/2022 5/9/2022 5 7 OK MW-65 Total Dissolved Solids 6/7/2022 6/10/2022 3 7 OK G-3A: Quarterly Sample Laboratory Receipt Temperature Check Sample Batch Wells in Batch Temperature GEL 576962 Nl\V-l,Nl\V-2,lvl\V-18,lvl\V-19,Nl\V-25,l\1\V-27,l\1\V-29, NA l\1\V-31,l\1\V-32,l\1\V-35, l\1\V-65 GEL 577764 l\1\V-5,Nl\V-ll,lvl\V-12,l\1\V-14,l\1\V-15,Nl\V-17,l\1\V-28, NA l\1\V-30, l\1\V-36, l\1\V-39, l\1\V-40, l\1\V-70 GEL 578558 N1\V-3A, l\1\V-22, l\1\V-23, l\1\V-24, N1\V-24A, lvl\V-26 NA Resample, l\1\V-38, T\V4-24 GEL 580437 l\1\V-20, l\1\V-37 NA CTF 22Dll97 Nl\V-l,l\1\V-2, lvl\V-18,l\1\V-19,l\1\V-25,lvl\V-27,lvl\V-29, 0.9 °C Nl\V-31, l\1\V-32, l\1\V-35, l\1\V-65, Trip Blank l\1\V-5,l\1\V-ll,l\1\V-12,l\1\V-14,l\1\V-15,Nl\V-17,lvl\V-26, CTF22D1691 l\1\V-28, l\1\V-30, l\1\V-36, l\1\V-39, l\1\V-40, l\1\V-70, Trip 0.9 °C Blank CTF 22D2139 l\1\V-3A, l\1\V-22, l\1\V-23, l\1\V-24, l\1\V-24A, l\1\V-38, T\V4-0.0 °C 24, Trip Blank CTF 22E1503 l\1\V-20, l\1\V-27 Resample, lvl\V-32 Resample, l\1\V-37 1.0 °C NIA== These shipments contained samples for the analysis of gross alpha or metals only. Per Table 1 in the approved QAP, samples submitted for gross alpha or metals analyses do not have a sample temperature requirement. G-3B: Accelerated Sample Laboratory Receipt Temperature Check Sample Batch Wens in Ba~cb Temperature CTF 22E0524 -May MW-11, MW-25, MW-26, MW-30, MW-31, MW-65, Trip 1.7 °C Blank CTF 22F0888 -June MW-11, MW-25, MW-26, MW-30, MW-31, MW-65, Trip 1.3 °c Blank G-4A: Quarterly Sample Analytical Method Check Parameter QAPMethod Method Used by Lab Ammonia (as N) A4500-NH3 G or E350.1 E350.1 Nitrate+ Nitrite (as N) E353.1 or E353.2 E353.2 Metals E200.7 or E200.8 E200.7 and E200.8 Gross Alpha E900.0 or E900. l or E903.0 E903.0 voes SW8260B or SW8260C or SW8260D SW8260D Chloride A4500-Cl B or A4500-Cl E or E300.0 E300.0 Fluoride A4500-F C or E300.0 E300.0 Sulfate A4500-S04 E or E300.0 E300.0 TDS A2540C A2540C Carbonate as C03, Bicarbonate as HC03 A2320 B A2320 B Mercury E245.1 or E200.7 or E200.8 E245.1 Calcium, Magnesium, Potassium, Sodium E200.7 E200.7 G-4B: Accelerated Sample Analytical Method Check Ptuamcter QAPMcthod Metl.1od Q.sed by. Lab Nitrate+ Nitrite (as N) E353. l or E353.2 E353.2 Metals E200.7 or E200.8 E200.7 or E200.8 voes SW8260B or SW8260C or SW8260D SW8260D Chloride A4500-Cl B or A4500-Cl E or E300.0 E300.0 Sulfate A4500-S04 E or E300.0 E300.0 TDS A2540C A2540C G 5AQ -1 S uarter1y ampe .eoortmg IR 1m1t ec L" . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check Trip Blank Acetone 20 ug/L u I 20 OK Trip Blank Benzene l ug/L u I I OK Trip Blank Carbon Tetrachloride I ug/L u I I OK Trip Blank Chloroform I ug/L u I 1 OK Trip Blank Chloromethane I ug/L u I 1 OK Trip Blank Methyl Ethyl Ketone 20 ug/L u I 20 OK Trip Blank Methylene Chloride 1 ug/L u I I OK Trip Blank Naphthalene I ug/L u I l OK Trip Blank Te1rahydrofuran I ug/L u I 1 OK Trip Blank Toluene 1 ug/L u I J OK Trip Blank Xylenes, total I ug/L u I l OK Trip Blank Acetone 20 ug/L u I 20 OK Trip Blank Benzene 1 ug/L u I I OK Trip Blank Carbon Tetrachloride I ug/L u I 1 OK Trip Blank Chloroform 1 ug/L u I I OK Trip Blank Chloromethane I ug/L u I I OK Trip Blank MeU1yl Ethyl Ketone 20 ug/L u I 20 OK Trip Blank Methylene Chloride I ug/L u 1 I OK Trip Blank Naphthalene I ug/L u 1 I OK Trip Blank Tetrahydrofuran I ug/L u I 1 OK Trip Blank Toluene I ug/L u I I OK Trip Blank Xylenes, total I ug/L u I 1 OK Trip Blank Acetone 20 ug/L u I 20 OK Trip Blank Benzene I ug/L u 1 I OK Trip Blank Carbon Tetrachloride 1 ug/L u I I OK Trip Blank Chloroform I ug/L u 1 1 OK Trip Blank Chloromethane I ug/L u 1 1 OK Trip Blank Methyl Ethyl Ketone 20 ug/L u 1 20 OK Trip Blank Methylene Chloride I ug/L u I 1 OK Trip Blank Naphthalene I ug/L u I I OK Trip Blank Tetrahydrofuran I ug/L u I 1 OK Trip Blank Toluene I ug/L u 1 1 OK Trip Blank Xylenes, total I ug/L u I 1 OK Trip Blank Acetone 20 ug/L u I 20 OK Trip Blank Benzene I ug/L u I I OK Trip Blank Carbon Tetrachloride I ug/L u I 1 OK Trip Blank Chloroform I ug/L u 1 I OK Trip Blank Chloromethane 1 ug/L u I 1 OK Trip Blank Methyl Ethyl Ketone 20 ug/L u I 20 OK Trip Blank Methylene Chloride I ug/L u I I OK Trip Blank Naphtlrnlene I ug/L u I I OK Trip Blank Tetrahydrofuran 1 ug/L u I I OK Trip Blank Toluene I ug/L u 1 I OK Trip Blank Xvlencs, total 1 ug/L u I I OK MW-01 Acetone 20 ug/L u I 20 OK MW-01 Arsenic 5 ug/L u I 5 OK MW-01 Benzene I ug/L u 1 1 OK MW-01 Beryllium 0.5 ug/L u I 0.5 OK MW-01 Bicarbonate as CaC03 1 mg/L I 1 OK MW-01 Cadmium 0.5 ug/L u I 0.5 OK MW-01 Calcium 0.2 mg/L I 0.5 OK MW-01 Carbon Tetrachloride I ug/L u I I OK MW-01 Carbonate as C03 1 mg/L u 1 1 OK MW-01 Chloride 5 mg/L 5 I OK G-5A Quarterly Sample Reporting Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-01 Chloroform I ug/L u I 1 OK MW-01 Chloromethane 1 ug/L u 1 1 OK MW-OJ Chromium 25 ug/L u 1 25 OK MW-01 Cobalt 10 ug/L u 1 JO OK MW-01 Copper 10 ug/L u 1 10 OK MW-01 Fluoride 0.1 mg/L I 0.1 OK MW-01 Gross Radium Alpha 0.831 pCi/L u 1 1 OK MW-01 Iron 30 ug/L 1 30 OK MW-01 Lead 1 ug/L u 1 1 OK MW-01 Magnesium 0.2 mg/L 1 0.5 OK MW-01 Man11:anese 10 ug/L 1 10 OK MW-01 Mercury 0.5 ug/L u 1 0.5 OK MW-01 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-01 Methylene Chloride 1 ug/L u 1 1 OK MW-01 Molybdenum 10 ug/L u 1 10 OK MW-01 Naphthalene I ug/L u I 1 OK MW-01 Nickel 20 ug/L u 1 20 OK MW-01 Nitrate + Nitrite as N 0.1 mg/L u 1 0.1 OK MW-01 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-01 Potassium 0.5 mg/L 1 0.5 OK MW-01 Selenium 5 ug/L u 1 5 OK MW-01 Silver 10 ug/L u 1 10 OK MW-01 Sodium 0.5 mg/L 1 0.5 OK MW-01 Sulfate 5 mg/L 5 1 OK MW-01 Tetrahvdrofuran 1 ug/L 1 1 OK MW-01 Thallium 0.5 ug/L u 1 0.5 OK MW-01 Tin 100 ug/L u 1 100 OK MW-01 Toluene 1 ug/L u 1 1 OK MW-01 Total Dissolved Solids 20 MG/L 1 10 OK MW-01 Uranium 0.3 ug/L u 1 0.3 OK MW-01 Vanadium 15 ug/L u 1 15 OK MW-01 Xylenes, total 1 ug/L u 1 1 OK MW-01 Zinc 10 ug/L u 1 10 OK MW-02 Acetone 20 ug/L u 1 20 OK MW-02 Arsenic 5 ug/L u 1 5 OK MW-02 Benzene 1 ug/L u 1 1 OK MW-02 Beryllium 0.5 ug/L u 1 0.5 OK MW-02 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-02 Cadmium 0.5 ug/L u 1 0.5 OK MW-02 Calcium 0.2 mg/L 1 0.5 OK MW-02 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-02 Carbonate as C03 1 mg/L u 1 1 OK MW-02 Chloride 5 mg/L 5 1 OK MW-02 Chloroform 1 ug/L u 1 1 OK MW-02 Chloromethane 1 ug/L u 1 1 OK MW-02 Chromium 25 ug/L u 1 25 OK MW-02 Cobalt 10 ug/L u 1 10 OK MW-02 Copper 10 ug/L u 1 10 OK MW-02 Fluoride 0.1 mg/L 1 0.1 OK MW-02 Gross Radium Alpha 0.686 pCi/L u 1 1 OK MW-02 Iron 30 ug/L u 1 30 OK MW-02 Lead 1 ug/L u 1 1 OK MW-02 Magnesium 0.2 mg/L 1 0.5 OK MW-02 Manganese 10 ug/L u 1 10 OK -G 5AQ uarter IY ample s I R eporlinJ?. 1m1t ec L" . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-02 Mercury 0.5 ug/L u 1 0.5 OK MW-02 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-02 Methylene Chloride 1 ug/L u 1 1 OK MW-02 Molybdenum 10 ug/L u 1 10 OK MW-02 Naphthalene 1 ug/L u 1 1 OK MW-02 Nickel 20 ug/L u 1 20 OK MW-02 Nitrate + Nitrite as N 0.1 mg/L u 1 0.1 OK MW-02 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-02 Potassium 0.5 mg/L 1 0.5 OK MW-02 Selenium 5 ug/L I 5 OK MW-02 Silver 10 ug/L u I 10 OK MW-02 Sodium 0.5 mg/L 1 0.5 OK MW-02 Sulfate 50 mg/L 50 1 OK MW-02 Tetrahydrofuran I ug/L u 1 1 OK MW-02 Thallium 0.5 ug/L u 1 0.5 OK MW-02 Tin 100 ug/L u 1 100 OK MW-02 Toluene 1 ug/L u 1 1 OK MW-02 Total Dissolved Solids 500 MG/L 1 10 OK MW-02 Uranium 0.5 ug/L 1 0.3 OK MW-02 Vanadium 15 ug/L u 1 15 OK MW-02 Xylenes, total 1 ug/L u 1 1 OK MW-02 Zinc 10 ug/L u 1 10 OK MW-03a Acetone 20 ug/L u I 20 OK MW-03a Arsenic 5 ug/L u 1 5 OK MW-03a Benzene 1 ug/L u 1 1 OK MW-03a Beryllium 0.5 ug/L u 1 0.5 OK MW-03a Bicarbonate as CaC03 1 mg/L 1 I OK MW-03a Cadmium 0.5 ug/L 1 0.5 OK MW-03a Calcium 0.4 mg/L 2 0.5 OK MW-03a Carbon Tetrachloride 1 ug/L u 1 I OK MW-03a Carbonate as C03 1 mg/L u 1 1 OK MW-03a Chloride 50 mg/L 50 1 OK MW-03a Chloroform 1 ug/L u I 1 OK MW-03a Chloromethane 1 ug/L u 1 I OK MW-03a Chromium 25 ug/L u 1 25 OK MW-03a Cobalt 10 ug/L u 1 10 OK MW-03a Copper 10 ug/L u 1 10 OK MW-03a Fluoride 0.1 mg/L u 1 0.1 OK MW-03a Gross Radium Alpha 0.917 pCi/L u I 1 OK MW-03a Iron 40 ug/L u 2 30 OK MW-03a Lead 1 ug/L u 1 1 OK MW-03a Magnesium 0.4 mg/L 2 0.5 OK MW-03a Manganese 10 ug/L 5 10 OK MW-03a Mercury 0.5 ug/L u 1 0.5 OK MW-03a Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-03a Methylene Chloride 1 ug/L u 1 I OK MW-03a Molybdenum 10 ug/L u 1 10 OK MW-03a Naphthalene 1 ug/L u 1 1 OK MW-03a Nickel 20 ug/L u 1 20 OK MW-03a Nitrate+ Nitrite as N 0.1 mg/L 1 0.1 OK MW-03a Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-03a Potassium 1 mg/L 2 0.5 OK MW-03a Selenium 5 ug/L 1 5 OK MW-03a Silver 10 ug/L u I 10 OK G 5AQ -I S I R uar1er1y amp e eoorung 1m1t ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analvte Limit Units Qualifier Factor Limit Check MW-03a Sodium I mg/L 2 0.5 OK MW-03a Sulfate 50 mg/L 50 1 OK MW-03a Tetrahydrofuran 1 ug/L u 1 1 OK MW-03a Thallium 0.2 ug/L 1 0.5 OK MW-03a Tin 100 ug/L u 2 100 OK MW-03a Toluene 1 ug/L u 1 1 OK MW-03a Total Dissolved Solids 20 MG/L 1 10 OK MW-03a Uranium 0.3 ug/L 1 0.3 OK MW-03a Vanadium 15 ug/L u l 15 OK MW-03a Xylenes, total 1 ug/L u l I OK MW-03a Zinc 10 ug/L l 10 OK MW-05 Acetone 20 ug/L u 1 20 OK MW-05 Arsenic 5 ug/L u l 5 OK MW-05 Benzene 1 ug/L u 1 1 OK MW-05 Beryllium 0.5 ug/L u l 0.5 OK MW-05 Bicarbonate as CaC03 l mg/L l 1 OK MW-05 Cadmium 0.5 ug/L u 1 0.5 OK MW-05 Calcium 0.2 mg/L I 0.5 OK MW-05 Carbon Tetrachloride 1 ug/L u 1 I OK MW-05 Carbonate as C03 I mg/L u 1 1 OK MW-05 Chloride 1 mg/L l 1 OK MW-05 Chloroform l ug/L u 1 1 OK MW-05 Ch loromethane l ug/L u l 1 OK MW-05 Chromium 25 ug/L u 1 25 OK MW-05 Cobalt 10 ug/L u 1 10 OK MW-05 Copper 10 ug/L u l 10 OK MW-05 Fluoride 0.1 mg/L 1 0.1 OK MW-05 Gross Radium Alpha 0.585 pCi/L u I 1 OK MW-05 Iron 30 ug/L u 1 30 OK MW-05 Lead 1 ug/L u 1 1 OK MW-05 Magnesium 0.2 mg/L l 0.5 OK MW-05 Manganese IO ug/L l 10 OK MW-05 Mercury 0.5 ug/L u l 0.5 OK MW-05 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-05 Methylene Chloride 1 ug/L u 1 1 OK MW-05 Molybdenum IO ug/L u l IO OK MW-05 Naphthalene 1 ug/L u 1 1 OK MW-05 Nickel 20 ug/L u 1 20 OK MW-05 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-05 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-05 Potassium 0.5 mg/L 1 0.5 OK MW-05 Selenium 5 ug/L u 1 5 OK MW-05 Silver 10 ug/L u 1 10 OK MW-05 Sodium 2.5 mg/L 5 0.5 OK MW-05 Sulfate 20 mg/L 20 I OK MW-05 Tetrahydrofuran 1 ug/L u 1 1 OK MW-05 Thallium 0.5 ug/L u 1 0.5 OK MW-05 Tin 100 ug/L u 1 JOO OK MW-05 Toluene 1 ug/L u 1 1 OK MW-05 Total Dissolved Solids 20 MG/L 1 10 OK MW-05 Uranium 0.5 ug/L 1 0.3 OK MW-05 Vanadium 15 ug/L u 1 15 OK MW-05 Xvlenes, total 1 ug/L u 1 l OK MW-05 Zinc IO ug/L u 1 10 OK G-5A Quarterly Sample Reportin.!1. Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-11 Acetone 20 ug/L u l 20 OK MW-11 Arsenic 5 ug/L u l 5 OK MW-11 Benzene 1 ug/L u 1 1 OK MW-11 Beryllium 0.5 ug/L u I 0.5 OK MW-11 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-11 Cadmium 0.5 ug/L u 1 0.5 OK MW-11 Calcium 0.2 mg/L 1 0.5 OK MW-11 Carbon Tetrachloride 1 ug/L u l I OK MW-11 Carbonate as C03 1 mg/L u 1 1 OK MW-11 Chloride 20 mg/L 20 I OK MW-11 Chloroform 1 ug/L u 1 1 OK MW-11 Chloromethane l ug/L u l 1 OK MW-11 Chromium 25 ug/L u 1 25 OK MW-11 Cobalt 10 ug/L u 1 10 OK MW-11 Coooer 10 ug/L u l 10 OK MW-11 Fluoride 0.1 mg/L l 0.1 OK MW-11 Gross Radium Alpha 0.712 pCi/L u 1 1 OK MW-11 Iron 30 ug/L u 1 30 OK MW-11 Lead 1 ug/L u l I OK MW-11 Magnesium 0.2 mg/L I 0.5 OK MW-11 Manganese 10 ug/L 1 10 OK MW-11 Mercury 0.5 ug/L u 1 0.5 OK MW-11 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-11 Methylene Chloride l ug/L u I 1 OK MW-11 Molybdenum 10 ug/L u l 10 OK MW-11 Naphthalene l ug/L u l 1 OK MW-11 Nickel 20 ug/L u 1 20 OK MW-11 Nitrate+ Nitrite as N 0.1 mg/L l 0.1 OK MW-11 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-11 Potassium 0.5 mg/L 1 0.5 OK MW-11 Selenium 5 ug/L 1 5 OK MW-11 Silver 10 ug/L u 1 10 OK MW-11 Sodium 0.5 mg/L I 0.5 OK MW-11 Sulfate 20 mg/L 20 1 OK MW-11 Tetrahydrofuran 1 ug/L u I I OK MW-11 Thallium 0.5 ug/L u l 0.5 OK MW-11 Tin 100 ug/L u l 100 OK MW-11 Toluene 1 ug/L u 1 1 OK MW-11 Total Dissolved Solids 20 MOIL l 10 OK MW-11 Uranium 0.5 ug/L 1 0.3 OK MW-11 Vanadium 15 ug/L u 1 15 OK MW-11 Xylenes, total l ug/L u 1 l OK MW-11 Zinc 10 ug/L u 1 10 OK MW-12 Acetone 20 ug/L u l 20 OK MW-12 Arsenic 5 ug/L u l 5 OK MW-12 Benzene 1 ug/L u 1 l OK MW-12 Beryllium 0.5 ug/L u 1 0.5 OK MW-12 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-12 Cadmium 0.5 ug/L u 1 0.5 OK MW-12 Calcium 0.2 mg/L 1 0.5 OK MW-12 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-12 Carbonate as C03 1 mg/L u 1 1 OK MW-12 Chloride 50 mg/L 50 1 OK MW-12 Chloroform 1 ug/L u 1 l OK G-5A Quarterly Sample Reponi.nJ! Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-12 Chloromethane 1 ug/L u 1 I OK MW-12 Chromium 25 ug/L u I 25 OK MW-12 Cobalt IO ug/L u I 10 OK MW-12 Copper 10 ug/L u 1 IO OK MW-12 Fluoride 0.1 mg/L 1 0.1 OK MW-12 Gross Radium Alpha 0.517 pCi/L u I 1 OK MW-12 Iron 30 ug/L u 1 30 OK MW-12 Lead I ug/L u I 1 OK MW-1 2 Magnesium 0.2 mg/L 1 0.5 OK MW-12 Manganese 10 ug/L 1 IO OK MW-12 Mercury 0.5 ug/L u I 0.5 OK MW-12 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-12 Methylene Chloride 1 ug/L u I I OK MW-12 Molybdenum IO ug/L u 1 IO OK MW-12 Naphthalene 1 ug/L u 1 1 OK MW-12 Nickel 20 ug/L u 1 20 OK MW-12 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-12 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-12 Potassium 0.5 mg/L 1 0.5 OK MW-12 Selenium 5 ug/L 1 5 OK MW-12 Silver IO ug/L u l IO OK MW-12 Sodium 0.5 mg/L 1 0.5 OK MW-12 Sulfate 50 mg/L 50 1 OK MW-12 Tetrahydrofuran 1 ug/L u 1 1 OK MW-12 Thallium 0.5 ug/L u 1 0.5 OK MW-12 Tin 100 ug/L u 1 100 OK MW-12 Toluene 1 ug/L u 1 1 OK MW-12 Total Dissolved Solids 20 MG/L 1 IO OK MW-12 Uranium 2.5 ug/L 5 0.3 OK MW-12 Vanadium 15 ug/L u 1 15 OK MW-12 Xylenes, total 1 ug/L u 1 1 OK MW-12 Zinc IO ug/L u 1 IO OK MW-14 Acetone 20 ug/L u 1 20 OK MW-14 Arsenic 5 ug/L u 1 5 OK MW-14 Benzene 1 ug/L u 1 1 OK MW-14 Beryllium 0.5 ug/L u 1 0.5 OK MW-14 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-14 Cadmium 0.5 ug/L 1 0.5 OK MW-14 Calcium 0.2 mg/L 1 0.5 OK MW-14 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-14 Carbonate as C03 1 mg/L u 1 1 OK MW-14 Chloride 1 mg/L 1 1 OK MW-14 Chloroform I ug/L u I 1 OK MW-14 Chloromethane 1 ug/L u I 1 OK MW-14 Chromium 25 ug/L u 1 25 OK MW-14 Cobalt IO ug/L u 1 IO OK MW-14 Copper IO ug/L u 1 IO OK MW-14 Fluoride 0.1 mg/L u 1 0.1 OK MW-14 Gross Radium Alpha 0.568 pCi/L u 1 1 OK MW-14 Iron 30 ug/L u 1 30 OK MW-14 Lead I ug/L u l l OK MW-14 Magnesium 0.2 mg/L 1 0.5 OK MW-14 Manganese 10 ug/L 1 10 OK MW-14 Mercury 0.5 ug/L u 1 0.5 OK G 5AQ -uanerly amp e I S IR epor11ng 1m1t ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-14 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-14 Methylene Chloride 1 ug/L u 1 1 OK MW-14 Molybdenum 10 ug/L u I 10 OK MW-14 Naphthalene 1 ug/L u 1 1 OK MW-14 Nickel 20 ug/L u 1 20 OK MW-14 Nitrate+ Nitrite as N 0.1 mg/L u 1 0.1 OK MW-14 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-14 Potassium 0.5 mg/L 1 0.5 OK MW-14 Selenium 5 ug/L u 1 5 OK MW-14 Silver 10 ug/L u 1 10 OK MW-14 Sodium 0.5 mg/L 1 0.5 OK MW-14 Sulfate 50 mg/L 50 1 OK MW-14 Tetrahydrofuran 1 ug/L u 1 1 OK MW-14 Thallium 0.5 ug/L u 1 0.5 OK MW-14 Tin 100 ug/L u 1 100 OK MW-14 Toluene I ug/L u 1 1 OK MW-14 Total Dissolved Solids 20 MG/L 1 JO OK MW-14 Uranium 0.3 ug/L 1 0.3 OK MW-14 Vanadium 15 ug/L u I 15 OK MW-14 Xylenes, total 1 ug/L u 1 I OK MW-14 Zinc 10 ug/L 1 10 OK MW-15 Acetone 20 ug/L u 1 20 OK MW-15 Arsenic 5 ug/L u 1 5 OK MW-15 Benzene 1 ug/L u 1 1 OK MW-15 Beryllium 0.5 ug/L u 1 0.5 OK MW-15 Bicarbonate as CaC03 I mg/L l I OK MW-15 Cadmium 0.5 ug/L u 1 0.5 OK MW-15 Calcium 0.2 mg/L I 0.5 OK MW-15 Carbon Tetrachloride I ug/L u 1 1 OK MW-15 Carbonate as C03 1 mg/L u 1 1 OK MW-15 Chloride 5 mg/L 5 I OK MW-15 Chloroform 1 ug/L u 1 1 OK MW-15 Chloromethane 1 ug/L u 1 1 OK MW-15 Chromium 25 ug/L u 1 25 OK MW-15 Cobalt 10 ug/L u 1 10 OK MW-15 Coooer 10 ug/L u 1 10 OK MW-15 Fluoride 0.1 mg/L A-Ola 5 0.1 OK MW-15 Gross Radium Alpha 0.631 pCi/L u 1 1 OK MW-15 Iron 30 ug/L u 1 30 OK MW-15 Lead 1 ug/L u 1 1 OK MW-15 Magnesium 0.2 mg/L 1 0.5 OK MW-15 Manganese 10 ug/L u 1 10 OK MW-15 Mercury 0.5 ug/L u 1 0.5 OK MW-15 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-15 Methylene Chloride 1 ug/L u 1 1 OK MW-15 Molybdenum 10 ug/L u 1 10 OK MW-15 Naphthalene 1 ug/L u 1 1 OK MW-15 Nickel 20 ug/L u 1 20 OK MW-15 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-15 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-15 Potassium 0.5 mg/L 1 0.5 OK MW-15 Selenium 5 ug/L 1 5 OK MW-15 Silver 10 ug/L u 1 10 OK MW-15 Sodium 0.5 mg/L 1 0.5 OK G-5A Quarterly Sample Reportfog Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-15 Sulfate 50 mg/L 50 1 OK MW-15 Tetrahvdrofuran 1 ug/L u 1 I OK MW-15 Thallium 0.5 uwl, u l 0.5 OK MW-15 Tin 100 ug/L u 1 100 OK MW-15 Toluene 1 ug/L u 1 I OK MW-15 Total Dissolved Solids 20 MG/L 1 IO OK MW-15 Uranium 2.5 ug/L 5 0.3 OK MW-15 Vanadium 15 ug/L u l 15 OK MW-15 Xylenes, total l ug/L u 1 1 OK MW-15 Zinc 10 ug/L u 1 10 OK MW-17 Acetone 20 ug/L u 1 20 OK MW-17 Arsenic 5 ug/L u 1 5 OK MW-17 Benzene 1 ug/L u 1 1 OK MW-17 Beryllium 0.5 ug/L u 1 0.5 OK MW-17 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-17 Cadmium 0.5 ug/L u 1 0.5 OK MW-17 Calcium 0.2 mg/L 1 0.5 OK MW-17 Carbon Tetrachloride l ug/L u l 1 OK MW-17 Carbonate as C03 1 mg/L u 1 1 OK MW-17 Chloride 1 mg/L 1 1 OK MW-17 Chloroform 1 ug/L u 1 1 OK MW-17 Chloromethane 1 ug/L u 1 1 OK MW-17 Chromium 25 ug/L u 1 25 OK MW-17 Cobalt 10 ug/L u 1 10 OK MW-17 Coooer 10 ug/L u 1 10 OK MW-17 Fluoride 0.1 mg/L 1 0.1 OK MW-17 Gross Radium Alpha 0.538 pCi/L u 1 1 OK MW-17 Iron 30 ug/L u 1 30 OK MW-17 Lead 1 ug/L u 1 1 OK MW-17 Magnesium 0.2 mg/L 1 0.5 OK MW-17 Manganese 10 ug/L 1 10 OK MW-17 Mercury 0.5 ug/L u 1 0.5 OK MW-17 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-17 Methylene Chloride 1 ug/L u 1 1 OK MW-17 Molybdenum 10 ug/L u 1 10 OK MW-17 Naphthalene 1 ug/L u 1 1 OK MW-17 Nickel 20 ug/L u 1 20 OK MW-17 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-17 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-17 Potassium 0.5 mg/L 1 0.5 OK MW-17 Selenium 5 ug/L 1 5 OK MW-17 Silver 10 ug/L u 1 10 OK MW-17 Sodium 0.5 mg/L 1 0.5 OK MW-17 Sulfate 50 mg/L 50 1 OK MW-17 Tetrahydrofuran 1 ug/L u 1 1 OK MW-17 Thallium 0.5 ug/L u 1 0.5 OK MW-17 Tin 100 ug/L u 1 100 OK MW-17 Toluene 1 ug/L u 1 1 OK MW-17 Total Dissolved Solids 20 MG/L 1 10 OK MW-17 Uranium 5 ug/L 10 0.3 OK MW-17 Vanadium 15 ug/L u 1 15 OK MW-17 Xylenes, total 1 ug/L u 1 1 OK MW-17 Zinc 10 ug/L u l 10 OK MW-18 Acetone 20 ug/L u l 20 OK G 5AQ -1 S I R uarterty amp e eporung 1m1t ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-18 Arsenic 5 ug/L u 1 5 OK MW-18 Benzene 1 ug/L u 1 1 OK MW-18 Beryllium 0.5 ug/L u l 0.5 OK MW-18 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-18 Cadmium 0.5 ug/L u 1 0.5 OK MW-18 Calcium 0.2 mg/L 1 0.5 OK MW-18 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-18 Carbonate as C03 1 mg/L u 1 1 OK MW-18 Chloride 5 mg/L 5 1 OK MW-18 Chloroform 1 ug/L u 1 1 OK MW-18 Chloromethane l ug/L u l l OK MW-18 Chromium 25 ug/L u l 25 OK MW-18 Cobalt 10 ug/L u l 10 OK MW-18 Copper 10 ug/L u 1 10 OK MW-18 Fluoride 0.1 mg/L 1 0.1 OK MW-18 Gross Radium Alpha 0.637 pCi/L u 1 l OK MW-18 Iron 30 ug/L u 1 30 OK MW-18 Lead l ug/L u l 1 OK MW-18 Magnesium 0.2 mg/L 1 0.5 OK MW-18 Manganese 10 ug/L l 10 OK MW-18 Mercury 0.5 ug/L u l 0.5 OK MW-18 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-18 Methylene Chloride l ug/L u 1 1 OK MW-18 Molybdenum 10 ug/L u 1 10 OK MW-18 Naphthalene l ug/L u l l OK MW-18 Nickel 20 ug/L u 1 20 OK MW-18 Nitrate+ Nitrite as N 0.1 mg/L u 1 0.1 OK MW-18 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-18 Potassium 0.5 mg/L 1 0.5 OK MW-18 Selenium 5 ug/L u 1 5 OK MW-18 Silver 10 ug/L u 1 10 OK MW-18 Sodium 0.5 mg/L 1 0.5 OK MW-18 Sulfate 50 mg/L 50 1 OK MW-18 Tetrahydrofuran 1 ug/L u 1 1 OK MW-18 Thallium 0.5 ug/L 1 0.5 OK MW-18 Tin 100 ug/L u 1 100 OK MW-18 Toluene 1 ug/L u 1 1 OK MW-18 Total Dissolved Solids 500 MG/L 1 10 OK MW-18 Uranium 0.5 ug/L 1 0.3 OK MW-18 Vanadium 15 ug/L u 1 15 OK MW-18 Xylenes, total 1 ug/L u 1 1 OK MW-18 Zinc 10 ug/L u 1 10 OK MW-19 Acetone 20 ug/L u 1 20 OK MW-19 Arsenic 5 ug/L u 1 5 OK MW-19 Benzene 1 ug/L u 1 1 OK MW-19 Beryllium 0.5 ug/L u 1 0.5 OK MW-19 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-19 Cadmium 0.5 ug/L u 1 0.5 OK MW-19 Calcium 0.2 mg/L 1 0.5 OK MW-19 Carbon Tetrachloride I ug/L u I I OK MW-19 Carbonate as C03 1 mg/L u 1 1 OK MW-19 Chloride 5 mg/L 5 1 OK MW-19 Chloroform 1 ug/L u 1 1 OK MW-19 Chloromethane 1 ug/L u I 1 OK G-5A Quarterly Sample Reportin_g Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-19 Chromium 25 ug/L u I 25 OK MW-I9 Cobalt IO ug/L u I IO OK MW-I9 Coooer IO ug/L u I IO OK MW-I9 Fluoride 0.5 mg/L 5 0.1 OK MW-19 Gross Radium Alpha 0.839 pCi/L u 1 1 OK MW-I9 Iron 30 ug/L u 1 30 OK MW-19 Lead 1 ug/L u 1 1 OK MW-19 Magnesium 0.2 mg/L 1 0.5 OK MW-19 Manganese IO ug/L u 1 10 OK MW-19 Mercury 0.5 ug/L u 1 0.5 OK MW-19 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-19 Methylene Chloride 1 ug/L u 1 1 OK MW-19 Molybdenum IO ug/L u 1 IO OK MW-19 Naphthalene 1 ug/L u 1 1 OK MW-19 Nickel 20 ug/L u 1 20 OK MW-19 Nitrate + Nitrite as N 0.1 mg/L I 0.1 OK MW-19 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-19 Potassium 0.5 mg/L 1 0.5 OK MW-19 Selenium 5 ug/L 1 5 OK MW-19 Silver IO ug/L u 1 IO OK MW-19 Sodium 0.5 mg/L I 0.5 OK MW-19 Sulfate 5 mg/L 5 1 OK MW-19 Tetrahydrofuran 1 ug/L u 1 1 OK MW-19 Thallium 0.5 ug/L u 1 0.5 OK MW-19 Tin 100 ug/L u 1 100 OK MW-I9 Toluene l ug/L u 1 1 OK MW-19 Total Dissolved Solids 500 MG/L 1 IO OK MW-19 Uranium 0.5 ug/L 1 0.3 OK MW-19 Vanadium 15 ug/L u 1 15 OK MW-19 Xylenes, total 1 ug/L u 1 1 OK MW-19 Zinc IO ug/L u 1 IO OK MW-20 Acetone 20 ug/L u 1 20 OK MW-20 Arsenic 5 UJl:/L u 1 5 OK MW-20 Benzene 1 ug/L u 1 1 OK MW-20 Beryllium 0.5 ug/L u 1 0.5 OK MW-20 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-20 Cadmium 0.5 ug/L u 1 0.5 OK MW-20 Calcium 1 mg/L 5 0.5 OK MW-20 Carbon Tetrachloride l ug/L u 1 1 OK MW-20 Carbonate as C03 1 mg/L u 1 1 OK MW-20 Chloride I mg/L 1 1 OK MW-20 Chloroform 1 ug/L u 1 1 OK MW-20 Chloromethane 1 ug/L u 1 1 OK MW-20 Chromium 25 ug/L u 1 25 OK MW-20 Cobalt IO ug/L u 1 IO OK MW-20 Copper IO ug/L u 1 10 OK MW-20 Fluoride 0.1 mg/L 1 0.1 OK MW-20 Gross Radium Alpha 0.558 pCi/L u I 1 OK MW-20 Iron 100 ug/L u 5 30 OK MW-20 Lead I ug/L u 1 1 OK MW-20 Magnesium 1 mg/L 5 0.5 OK MW-20 Manganese 10 ug/L u I 10 OK MW-20 Mercury 0.5 ug/L u 1 0.5 OK MW-20 Methyl Ethyl Ketone 20 ug/L u I 20 OK G 5AQ -I S I R uanerty amp e eporl111g 1m1t ec L' . Ch k Lab Required !I Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-20 Methylene Chloride 1 ug/L u I 1 OK MW-20 Molybdenum JO ug/L 1 JO OK MW-20 Naphthalene 1 ug/L u I 1 OK MW-20 Nickel 20 ug/L u I 20 OK MW-20 Nitrate+ Nitrite as N 0.5 mg/L 5 0.1 OK MW-20 Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-20 Potassium 2.5 mg/L 5 0.5 OK MW-20 Selenium 5 ug/L u 1 5 OK MW-20 Silver 10 ug/L u 1 JO OK MW-20 Sodium 2.5 mg/L 5 0.5 OK MW-20 Sulfate JOO mg/L 100 I OK MW-20 Tetrahydrofuran I ug/L u I I OK MW-20 Thallium 0.2 ug/L u I 0.5 OK MW-20 Tin JOO ug/L u 5 JOO OK MW-20 Toluene 1 ug/L u 1 1 OK MW-20 Total Dissolved Solids 20 MG/L 1 10 OK MW-20 Uranium 0.3 ug/L 1 0.3 OK MW-20 Vanadium 15 ug/L u I 15 OK MW-20 Xylenes, total 1 ug/L u I I OK MW-20 Zinc JO ug/L u I 10 OK MW-22 Acetone 20 ug/L u 1 20 OK MW-22 Arsenic 5 ug/L u 1 5 OK MW-22 Benzene 1 ug/L u I I OK MW-22 Beryllium 0.5 ug/L 1 0.5 OK MW-22 Bicarbonate as CaC03 1 mg/L u 1 1 OK MW-22 Cadmium 0.5 ug/L 1 0.5 OK MW-22 Calcium 1 mg/L 5 0.5 OK MW-22 Carbon Tetrachloride 1 ug/L u 1 I OK MW-22 Carbonate as C03 1 mg/L u I 1 OK MW-22 Chloride 20 mg/L 20 1 OK MW-22 Chloroform 1 ug/L u 1 1 OK MW-22 Chloromethane I ug/L u 1 1 OK MW-22 Chromium 25 ug/L u 1 25 OK MW-22 Cobalt JO ug/L 1 JO OK MW-22 Copper 10 ug/L I 10 OK MW-22 Fluoride 0.1 mg/L 1 0.1 OK MW-22 Gross Radium Alpha 0.724 pCi/L 1 1 OK MW-22 Iron 100 ug/L 5 30 OK MW-22 Lead 1 ug/L 1 1 OK MW-22 Magnesium 1 mg/L 5 0.5 OK MW-22 Manganese 25 ug/L 50 10 OK MW-22 Mercury 0.5 ug/L u 1 0.5 OK MW-22 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-22 Methylene Chloride 1 ug/L u 1 1 OK MW-22 Molybdenum 10 ug/L 1 10 OK MW-22 Naphthalene 1 ug/L u 1 1 OK MW-22 Nickel 20 ug/L 1 20 OK MW-22 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-22 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-22 Potassium 2.5 mg/L 5 0.5 OK MW-22 Selenium 5 ug/L 1 5 OK MW-22 Silver 10 ug/L u 1 10 OK MW-22 Sodium 2.5 mg/L 5 0.5 OK MW-22 Sulfate 100 mg/L 100 1 OK G 5AQ -uaner :y amp e I S JR eport111g Ifill ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-22 Tetrahydrofuran 1 ug/L u 1 1 OK MW-22 Thallium 0.2 ug/L 1 0.5 OK MW-22 Tin 100 ug/L u 5 100 OK MW-22 Toluene 1 ug/L u 1 1 OK MW-22 Total Dissolved Solids 100 MG/L I 10 OK MW-22 Uranium 0.3 ug/L I 0.3 OK MW-22 Vanadium 15 ug/L u I 15 OK MW-22 Xylenes, total I ug/L u I I OK MW-22 Zinc 10 ug/L 1 10 OK MW-23 Acetone 20 ug/L u 1 20 OK MW-23 Arsenic 5 UJl:/L u I 5 OK MW-23 Benzene 1 ug/L u I 1 OK MW-23 Beryllium 0.5 ug/L u I 0.5 OK MW-23 Bicarbonate as CaC03 1 mg/L I I OK MW-23 Cadmium 0.5 ug/L u I 0.5 OK MW-23 Calcium 0.2 mg/L 1 0.5 OK MW-23 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-23 Carbonate as C03 1 mg/L u I I OK MW-23 Chloride I mg/L 1 I OK MW-23 Chloroform I ug/L u 1 I OK MW-23 Chloromethane I ug/L u 1 I OK MW-23 Chromium 25 ug/L u I 25 OK MW-23 Cobalt 10 ug/L u I 10 OK MW-23 Coooer 10 ug/L u I 10 OK MW-23 Fluoride 0.1 mg/L I 0.1 OK MW-23 Gross Radium Alpha 0.689 pCi/L u 1 I OK MW-23 Iron 30 ug/L u 1 30 OK MW-23 Lead 1 uwl, u I I OK MW-23 Ma)l;nesium 0.2 mg/L l 0.5 OK MW-23 Manganese 10 ug/L u 5 10 OK MW-23 Mercury 0.5 ug/L u 1 0.5 OK MW-23 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-23 Methylene Chloride I ug/L u I I OK MW-23 Molybdenum 10 ug/L u l 10 OK MW-23 Naphthalene 1 ug/L u 1 I OK MW-23 Nickel 20 ug/L u l 20 OK MW-23 Nitrate + Nitrite as N 0.1 mg/L I 0.1 OK MW-23 Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-23 Potassium 0.5 IDJl:/L 1 0.5 OK MW-23 Selenium 5 ug/L u 1 5 OK MW-23 Silver 10 ug/L u 1 10 OK MW-23 Sodium 0.5 mg/L 1 0.5 OK MW-23 Sulfate 100 mwL 100 I OK MW-23 Tetrahydrofuran 1 ug/L u 1 I OK MW-23 Thallium 0.2 ug/L I 0.5 OK MW-23 Tin 100 ug/L u 1 100 OK MW-23 Toluene 1 ug/L u 1 1 OK MW-23 Total Dissolved Solids 20 MG/L 1 10 OK MW-23 Uranium 0.3 ug/L 1 0.3 OK MW-23 Vanadium 15 ug/L u 1 15 OK MW-23 Xylenes, total 1 ug/L u l I OK MW-23 Zinc 10 ug/L u 1 10 OK MW-24 Acetone 20 ug/L u 1 20 OK MW-24 Arsenic 5 ug/L u I 5 OK G 5AQ -uarterly ample s IR eporung Limit Chee k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-24 Benzene l ug/L u 1 1 OK MW-24 Beryllium 0.5 ug/L 1 0.5 OK MW-24 Bicarbonate as CaC03 1 mg/L u 1 1 OK MW-24 Cadmium 0.5 ug/L 1 0.5 OK MW-24 Calcium 1 mg/L 5 0.5 OK MW-24 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-24 Carbonate as C03 l mg/L u 1 1 OK MW-24 Chloride 10 mg/L 10 1 OK MW-24 Chloroform 1 ug/L u 1 1 OK MW-24 Chloromethane 1 ug/L u 1 1 OK MW-24 Chromium 25 ug/L u l 25 OK MW-24 Cobalt 10 ug/L 1 10 OK MW-24 Copper 10 ug/L 1 10 OK MW-24 Fluoride 0.1 mg/L 1 0.1 OK MW-24 Gross Radium Alpha 0.666 pCi/L 1 1 OK MW-24 Iron 30 ug/L u 1 30 OK MW-24 Lead 1 ug/L 1 1 OK MW-24 Magnesium 0.2 mg/L 1 0.5 OK MW-24 Manganese 10 ug/L 5 10 OK MW-24 Mercury 0.5 ug/L u 1 0.5 OK MW-24 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-24 Methylene Chloride 1 ug/L u 1 1 OK MW-24 Molybdenum 10 ug/L u 1 10 OK MW-24 Naphthalene 1 ug/L u 1 1 OK MW-24 Nickel 20 ug/L 1 20 OK MW-24 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-24 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-24 Potassium 0.5 mg/L 1 0.5 OK MW-24 Selenium 5 ug/L 1 5 OK MW-24 Silver 10 ug/L u 1 10 OK MW-24 Sodium 0.5 mg/L 1 0.5 OK MW-24 Sulfate 50 mg/L 50 1 OK MW-24 Tetrahydrofuran 1 ug/L u 1 1 OK MW-24 Thallium 0.2 ug/L 1 0.5 OK MW-24 Tin 100 ug/L u 1 100 OK MW-24 Toluene 1 ug/L u 1 1 OK MW-24 Total Dissolved Solids 20 MG/L 1 10 OK MW-24 Uranium 0.3 ug/L 1 0.3 OK MW-24 Vanadium 15 ug/L u 1 15 OK MW-24 Xylenes, total 1 ug/L u 1 1 OK MW-24 Zinc 10 ug/L 1 10 OK MW-24A Acetone 20 ug/L u 1 20 OK MW-24A Arsenic 5 ug/L u 1 5 OK MW-24A Benzene 1 ug/L u 1 1 OK MW-24A Beryllium 0.5 ug/L 1 0.5 OK MW-24A Bicarbonate as CaC03 1 mg/L u I I OK MW-24A Cadmium 0.5 ug/L I 0.5 OK MW-24A Calcium I mg/L 5 0.5 OK MW-24A Carbon Tetrachloride 1 ug/L u I 1 OK MW-24A Carbonate as C03 1 mg/L u 1 1 OK MW-24A Chloride 10 mg/L 10 1 OK MW-24A Chloroform 1 ug/L u 1 1 OK MW-24A Chloromethane 1 ug/L u 1 1 OK MW-24A Chromium 25 ug/L u 1 25 OK G5AQ -uruter.y amp e :eoorlmg I S I R Ifill ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-24A Cobalt 10 ug/L 1 10 OK MW-24A Copper 10 ug/L 1 10 OK MW-24A Fluoride 0.1 mg/L l 0.1 OK MW-24A Gross Radium Alpha 0.563 pCi/L l l OK MW-24A Iron 30 ug/L u 1 30 OK MW-24A Lead 1 ug/L u 1 l OK MW-24A Magnesium 0.2 mg/L 1 0.5 OK MW-24A Manganese 10 ug/L 5 10 OK MW-24A Mercury 0.5 ug/L u 1 0.5 OK MW-24A Methyl Ethyl Ketone 20 ug/L u l 20 OK MW-24A Methylene Chloride 1 ug/L u 1 1 OK MW-24A Molybdenum 10 ug/L u 1 10 OK MW-24A Naphthalene I ug/L u 1 I OK MW-24A Nickel 20 ug/L 1 20 OK MW-24A Nitrate+ Nitrite as N 0.1 mg/L 1 0.1 OK MW-24A Nitrogen, Ammonia as N 0.05 mg/L I 0.05 OK MW-24A Potassium 0.5 mg/L I 0.5 OK MW-24A Selenium 5 ug/L 1 5 OK MW-24A Silver 10 ug/L u 1 10 OK MW-24A Sodium 0.5 mg/L 1 0.5 OK MW-24A Sulfate 50 mg/L 50 1 OK MW-24A Tetrahydrofuran J ug/L u 1 1 OK MW-24A Thallium 0.2 ug/L I 0.5 OK MW-24A Tin 100 ug/L u 1 JOO OK MW-24A Toluene I ug/L u 1 I OK MW-24A Total Dissolved Solids 20 MG/L 1 10 OK MW-24A Uranium 0.3 ug/L 1 0.3 OK MW-24A Vanadium 15 ug/L u 1 15 OK MW-24A Xylenes, total 1 ug/L u 1 1 OK MW-24A Zinc 10 ug/L 1 JO OK MW-25 Acetone 20 ug/L u 1 20 OK MW-25 Arsenic 5 ug/L u I 5 OK MW-25 Benzene 1 ug/L u 1 I OK MW-25 Beryllium 0.5 ug/L u 1 0.5 OK MW-25 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-25 Cadmium 0.5 ug/L 1 0.5 OK MW-25 Calcium 0.2 mg/L I 0.5 OK MW-25 Carbon Tetrachloride 1 ug/L u I 1 OK MW-25 Carbonate as C03 1 mg/L u 1 I OK MW-25 Chloride 5 mg/L 5 1 OK MW-25 Chloroform 1 ug/L u 1 1 OK MW-25 Chloromethane I ug/L u 1 I OK MW-25 Chromium 25 ug/L u 1 25 OK MW-25 Cobalt 10 ug/L u 1 10 OK MW-25 Coooer 10 ug/L u I 10 OK MW-25 Fluoride 0.1 mg/L I 0.1 OK MW-25 Gross Radium Alpha 0.698 pCi/L u 1 1 OK MW-25 Iron 30 ug/L u 1 30 OK MW-25 Lead 1 ug/L u 1 1 OK MW-25 Magnesium 0.2 mg/L 1 0.5 OK MW-25 Manganese 10 ug/L 1 10 OK MW-25 Mercury 0.5 ug/L u 1 0.5 OK MW-25 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-25 Methylene Chloride 1 ug/L u 1 I OK G5AQ -IR uarrerly Samp e eport1ng Limit C 1ec k Lab Required Reporting Dilution Reporting RL Location Analvte Limit Units Qualifier Factor Limit Check MW-25 Molybdenum IO ug/L 1 10 OK MW-25 Naphthalene I ug/L u I I OK MW-25 Nickel 20 ug/L u l 20 OK MW-25 Nitrate + Nitrite as N 0.1 mg/L u I 0.1 OK MW-25 Nitrogen, Ammonia as N 0.2 mg/L I 0.05 OK MW-25 Potassium 0.5 mg/L 1 0.5 OK MW-25 Selenium 5 ug/L u I 5 OK MW-25 Silver IO ug/L u I 10 OK MW-25 Sodium 0.5 mg/L I 0.5 OK MW-25 Sulfate 50 mg/L 50 I OK MW-25 Tetrahydrofuran 1 ug/L u 1 1 OK MW-25 Thallium 0.5 ug/L I 0.5 OK MW-25 Tin 100 ug/L u 1 100 OK MW-25 Toluene 1 ug/L u 1 1 OK MW-25 Total Dissolved Solids 500 MG/L I 10 OK MW-25 Uranium 0.5 ug/L I 0.3 OK MW-25 Vanadium 15 ug/L u 1 15 OK MW-25 Xylenes, total 1 ug/L u l l OK MW-25 Zinc 10 ug/L u 1 10 OK MW-26 Acetone 20 ug/L u 1 20 OK MW-26 Arsenic 5 ug/L u 1 5 OK MW-26 Benzene 1 ug/L u l 1 OK MW-26 Beryllium 0.5 ug/L u 1 0.5 OK MW-26 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-26 Cadmium 0.5 ug/L I 0.5 OK MW-26 Calcium 0.2 mg/L l 0.5 OK MW-26 Carbon Tetrachloride I ug/L u I 1 OK MW-26 Carbonate as C03 1 mg/L u 1 1 OK MW-26 Chloride 50 mg/L 50 1 OK MW-26 Chloroform IO ug/L 10 1 OK MW-26 Chloromethane 1 ug/L u l l OK MW-26 Chromium 25 ug/L u I 25 OK MW-26 Cobalt 10 ug/L u I IO OK MW-26 Coooer IO ug/L u l 10 OK MW-26 Fluoride 0.1 mg/L 1 0.1 OK MW-26 Iron 30 ug/L I 30 OK MW-26 Lead l ug/L u l 1 OK MW-26 Magnesium 0.2 mg/L I 0.5 OK MW-26 Manganese IO ug/L l 10 OK MW-26 Mercury 0.5 ug/L u 1 0.5 OK MW-26 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-26 Methylene Chloride 1 ug/L u l l OK MW-26 Molybdenum 10 ug/L u l 10 OK MW-26 Naphthalene 1 ug/L u 1 1 OK MW-26 Nickel 20 ug/L u I 20 OK MW-26 Nitrate + Nitrite as N 0.1 mg/L I 0.1 OK MW-26 Nitrogen, Ammonia as N 0.05 mg/L l 0.05 OK MW-26 Potassium 0.5 mg/L I 0.5 OK MW-26 Selenium 5 ug/L 1 5 OK MW-26 Silver IO ug/L u l 10 OK MW-26 Sodium 0.5 mg/L I 0.5 OK MW-26 Sulfate 50 mg/L 50 l OK MW-26 Tetrahydrofuran 1 ug/L u 1 1 OK MW-26 Thallium 0.5 ug/L u l 0.5 OK G5AQ -uarteriy amp: e I S l R eporung 1m1t ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-26 Tin 100 ug/L u 1 100 OK MW-26 Toluene 1 ug/L u 1 1 OK MW-26 Total Dissolved Solids 20 MG/L 1 10 OK MW-26 Uranium 2.5 ug/L 5 0.3 OK MW-26 Vanadium 15 ug/L u 1 15 OK MW-26 X ylenes, total l ug/L u 1 1 OK MW-26 Zinc 10 ug/L u 1 10 OK MW-26 Gross Radium Alpha 0.636 pCi/L u 1 1 OK MW-27 Acetone 20 ug/L u 1 20 OK MW-27 Arsenic 5 ug/L u 1 5 OK MW-27 Benzene 1 ug/L u 1 1 OK MW-27 Beryllium 0.5 ug/L u 1 0.5 OK MW-27 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-27 Cadmium 0.5 ug/L u 1 0.5 OK MW-27 Calcium 0.2 mg/L 1 0.5 OK MW-27 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-27 Carbonate as C03 1 mg/L u 1 1 OK MW-27 Chloride 5 mg/L 5 1 OK MW-27 Chloroform 1 ug/L u 1 1 OK MW-27 Chloromethane 1 ug/L u 1 1 OK MW-27 Chromium 25 ug/L u 1 25 OK MW-27 Cobalt 10 ug/L u 1 10 OK MW-27 Copper 10 ug/L u 1 10 OK MW-27 Fluoride 0.5 mg/L 5 0.1 OK MW-27 Gross Radium Alpha 0.913 pCi/L 1 1 OK MW-27 Iron 30 ug/L u 1 30 OK MW-27 Lead 1 ug/L u 1 1 OK MW-27 Magnesium 0.2 mg/L 1 0.5 OK MW-27 Manganese 10 ug/L u 1 10 OK MW-27 Mercury 0.5 ug/L u 1 0.5 OK MW-27 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-27 Methylene Chloride 1 ug/L u 1 1 OK MW-27 Molybdenum 10 ug/L u 1 10 OK MW-27 Naphthalene 1 ug/L u 1 1 OK MW-27 Nickel 20 ug/L u 1 20 OK MW-27 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-27 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-27 Potassium 0.5 mg/L 1 0.5 OK MW-27 Selenium 5 ug/L 1 5 OK MW-27 Silver 10 ug/L u 1 10 OK MW-27 Sodium 0.5 mg/L 1 0.5 OK MW-27 Sulfate 5 mg/L 5 1 OK MW-27 Tetrahydrofuran 1 ug/L u 1 1 OK MW-27 Thallium 0.5 ug/L u 1 0.5 OK MW-27 Tin 100 ug/L u 1 100 OK MW-27 Toluene 1 ug/L u 1 1 OK MW-27 Uranium 0.5 ug/L 1 0.3 OK MW-27 Vanadium 15 ug/L u 1 15 OK MW-27 Xylenes, total 1 ug/L u 1 1 OK MW-27 Zinc 10 ug/L u 1 10 OK MW-27 Total Dissolved Solids 20 MG/L 1 10 OK MW-28 Acetone 20 ug/L u 1 20 OK MW-28 Arsenic 5 ug/L 1 5 OK MW-28 Benzene 1 ug/L u 1 1 OK G 5AQ -uarler1y amp e 1 S 1 R eporung 1m1t ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-28 Beryllium 0.5 ug/L u 1 0.5 OK MW-28 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-28 Cadmium 0.5 ug/L 1 0.5 OK MW-28 Calcium 0.2 mg/L 1 0.5 OK MW-28 Carbon Tetrachloride I ug/L u I I OK MW-28 Carbonate as C03 1 mg/L u I I OK MW-28 Chloride 50 mg/L 50 I OK MW-28 Chloroform I u_g/L u I 1 OK MW-28 Chloromethane 1 ug/L u 1 1 OK MW-28 Chromium 25 ug/L u I 25 OK MW-28 Cobalt 10 ug/L 1 10 OK MW-28 Coooer 10 ug/L u 1 10 OK MW-28 Fluoride 0.1 mg/L 1 0.1 OK MW-28 Gross Radium Alpha 0.782 pCi/L u I 1 OK MW-28 Iron 30 ug/L u 1 30 OK MW-28 Lead 1 ug/L u I I OK MW-28 Magnesium 0.2 mg/L 1 0.5 OK MW-28 Manganese 10 ug/L I 10 OK MW-28 Mercury 0.5 ug/L u I 0.5 OK MW-28 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-28 Methylene Chloride I ug/L u I 1 OK MW-28 Molybdenum 10 ug/L u I 10 OK MW-28 Naphthalene I u,g/L u 1 I OK MW-28 Nickel 20 ug/L u I 20 OK MW-28 Nitrate + Nitrite as N 0.1 mg/L I 0.1 OK MW-28 Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-28 Potassium 0.5 mg/L 1 0.5 OK MW-28 Selenium 5 ug/L I 5 OK MW-28 Silver 10 ug/L u I 10 OK MW-28 Sodium 0.5 mg/L I 0.5 OK MW-28 Sulfate 50 mg/L 50 I OK MW-28 Tetrahydrofuran 1 ug/L u 1 1 OK MW-28 Thallium 0.5 ug/L I 0.5 OK MW-28 Tin 100 ug/L u 1 100 OK MW-28 Toluene 1 ug/L u 1 I OK MW-28 Total Dissolved Solids 20 MG/L I 10 OK MW-28 Uranium 2.5 ug/L 5 0.3 OK MW-28 Vanadium 15 ug/L u I 15 OK MW-28 Xylenes, total 1 ug/L u 1 1 OK MW-28 Zinc 10 ug/L 1 10 OK MW-29 Acetone 20 ug/L u 1 20 OK MW-29 Arsenic 5 ug/L u 1 5 OK MW-29 Benzene 1 ug/L u 1 1 OK MW-29 Beryllium 0.5 ug/L u I 0.5 OK MW-29 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-29 Cadmium 0.5 ug/L u 1 0.5 OK MW-29 Calcium 0.2 mg/L 1 0.5 OK MW-29 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-29 Carbonate as C03 1 mg/L u 1 1 OK MW-29 Chloride 5 mg/L 5 1 OK MW-29 Chloroform 1 ug/L u 1 1 OK MW-29 Chloromethane 1 ug/L u 1 1 OK MW-29 Chromium 25 ug/L u 1 25 OK MW-29 Cobalt 10 ug/L u 1 10 OK G5AQ -I S I R uaner1y amp e eporlmg 1m1t ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-29 Copper 10 ug/L u 1 10 OK MW-29 Fluoride 0.5 mg/L 5 0.1 OK MW-29 Gross Radium Alpha 0.869 pCi/L u l l OK MW-29 Iron 30 ug/L 1 30 OK MW-29 Lead 1 ug/L u 1 1 OK MW-29 Magnesium 0.2 mg/L 1 0.5 OK MW-29 Manganese 10 ug/L 5 10 OK MW-29 Mercury 0.5 ug/L u I 0.5 OK MW-29 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-29 Methylene Chloride 1 ug/L u 1 I OK MW-29 Molybdenum 10 ug/L u 1 10 OK MW-29 Naphthalene l ug/L u 1 I OK MW-29 Nickel 20 ug/L u 1 20 OK MW-29 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-29 Nitrogen, Ammonia as N 0.2 mg/L l 0.05 OK MW-29 Potassium 0.5 mg/L l 0.5 OK MW-29 Selenium 5 ug/L u 1 5 OK MW-29 Silver 10 ug/L u l 10 OK MW-29 Sodium 0.5 mg/L 1 0.5 OK MW-29 Sulfate 50 mg/L 50 I OK MW-29 Tetrahydrofuran 1 ug/L u 1 I OK MW-29 Thallium 0.5 ug/L u 1 0.5 OK MW-29 Tin 100 ug/L u 1 100 OK MW-29 Toluene 1 ug/L u 1 1 OK MW-29 Total Dissolved Solids 20 MG/L 1 10 OK MW-29 Uranium 0.5 ug/L 1 0.3 OK MW-29 Vanadium 15 ug/L u l 15 OK MW-29 Xylenes, total 1 ug/L u I 1 OK MW-29 Zinc 10 ug/L u 1 10 OK MW-30 Acetone 20 ug/L u 1 20 OK MW-30 Arsenic 5 ug/L u 1 5 OK MW-30 Benzene 1 ug/L u 1 1 OK MW-30 Beryllium 0.5 ug/L u I 0.5 OK MW-30 Bicarbonate as CaC03 1 mg/L l 1 OK MW-30 Cadmium 0.5 ug/L u 1 0.5 OK MW-30 Calcium 0.2 mg/L 1 0.5 OK MW-30 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-30 Carbonate as C03 1 mg/L u I l OK MW-30 Chloride 50 mg/L 50 1 OK MW-30 Chloroform l ug/L u 1 I OK MW-30 Chloromethane 1 ug/L u 1 1 OK MW-30 Chromium 25 ug/L u 1 25 OK MW-30 Cobalt 10 ug/L u l 10 OK MW-30 Cooner 10 ug/L u 1 10 OK MW-30 Fluoride 0.1 mg/L 1 0.1 OK MW-30 Gross Radium Alpha 0.532 pCi/L u 1 1 OK MW-30 Iron 30 ug/L u 1 30 OK MW-30 Lead 1 ug/L u 1 l OK MW-30 Magnesium 0.2 mg/L 1 0.5 OK MW-30 Manganese 10 ug/L u 1 10 OK MW-30 Mercury 0.5 ug/L u 1 0.5 OK MW-30 Methyl Ethyl Ketone 20 ug/L u l 20 OK MW-30 Methylene Chloride 1 ug/L u I 1 OK MW-30 Molybdenum 10 ug/L u 1 10 OK G 5AQ -I S I R uar1er1 y amp! e eporung 1m1t ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-30 Naphthalene 1 ug/L u 1 I OK MW-30 Nickel 20 ug/L u 1 20 OK MW-30 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-30 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-30 Potassium 0.5 mg/L 1 0.5 OK MW-30 Selenium 5 ug/L 1 5 OK MW-30 Silver 10 ug/L u I 10 OK MW-30 Sodium 0.5 mg/L 1 0.5 OK MW-30 Sulfate 50 mg/L 50 I OK MW-30 Tetrahydrofuran I ug/L u l 1 OK MW-30 Thallium 0.5 ug/L u 1 0.5 OK MW-30 Tin 100 ug/L u 1 100 OK MW-30 Toluene 1 ug/L u 1 I OK MW-30 Total Dissolved Solids 20 MG/L 1 10 OK MW-30 Uranium 2.5 ug/L 5 0.3 OK MW-30 Vanadium 15 ug/L u 1 15 OK MW-30 Xylenes, total 1 ug/L u 1 1 OK MW-30 Zinc 10 ug/L u I 10 OK MW-31 Acetone 20 ug/L u 1 20 OK MW-31 Arsenic 5 ug/L u 1 5 OK MW-31 Benzene 1 ug/L u 1 1 OK MW-31 Beryllium 0.5 ug/L u 1 0.5 OK MW-31 Bicarbonate as CaC03 I mg/L 1 I OK MW-31 Cadmium 0.5 ug/L u 1 0.5 OK MW-31 Calcium 0.2 mg/L I 0.5 OK MW-31 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-31 Carbonate as C03 1 mg/L u I 1 OK MW-31 Chloride 20 mg/L 20 1 OK MW-31 Chloroform 1 ug/L u 1 1 OK MW-31 Chloromethane 1 ug/L u 1 I OK MW-31 Chromium 25 ug/L u 1 25 OK MW-31 Cobalt 10 ug/L u i 10 OK MW-31 Copper 10 ug/L u I 10 OK MW-31 Fluoride 0.1 mg/L 1 0.1 OK MW-31 Gross Radium Alpha 0.77 pCi/L u 1 1 OK MW-31 Iron 30 ug/L u 1 30 OK MW-31 Lead 1 ug/L u 1 I OK MW-31 Magnesium 0.2 mg/L 1 0.5 OK MW-31 Manganese 10 ug/L u 1 10 OK MW-31 Mercury 0.5 ug/L u 1 0.5 OK MW-31 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-31 Methylene Chloride 1 ug/L u 1 1 OK MW-31 Molybdenum 10 ug/L u l 10 OK MW-31 Naphthalene 1 ug/L u 1 l OK MW-31 Nickel 20 ug/L u 1 20 OK MW-31 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-31 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-31 Potassium 0.5 mg/L 1 0.5 OK MW-31 Selenium 5 ug/L 1 5 OK MW-31 Silver 10 ug/L u 1 10 OK MW-31 Sodium 0.5 mg/L 1 0.5 OK MW-31 Sulfate 20 mg/L 20 I OK MW-31 Tetrahydrofuran 1 ug/L u 1 1 OK MW-31 Thallium 0.5 ug/L u 1 0.5 OK G5AQ -l S I R uarten v amp e eportmg 1m1t ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-31 Tin 100 ug/L u I 100 OK MW-31 Toluene I ug/L u 1 I OK MW-31 Total Dissolved Solids 500 MG/L 1 10 OK MW-31 Uranium 0.5 ug/L 1 0.3 OK MW-31 Vanadium 15 ug/L u 1 15 OK MW-31 Xylenes, total 1 ug/L u 1 I OK MW-31 Zinc IO ug/L u 1 10 OK MW-32 Acetone 20 ug/L u 1 20 OK MW-32 Arsenic 5 ug/L u I 5 OK MW-32 Benzene 1 ug/L u 1 1 OK MW-32 Beryllium 0.5 ug/L u 1 0.5 OK MW-32 Bicarbonate as CaC03 1 mg/L 1 I OK MW-32 Cadmium 0.5 ug/L 1 0.5 OK MW-32 Calcium 2 mg/L 10 0.5 OK MW-32 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-32 Carbonate as C03 1 mg/L u I 1 OK MW-32 Chloride 5 mg/L 5 I OK MW-32 Chloroform 1 ug/L u 1 1 OK MW-32 Chloromethane 1 ug/L u 1 1 OK MW-32 Chromium 25 ug/L u 1 25 OK MW-32 Cobalt 10 ug/L 1 10 OK MW-32 Copper 10 ug/L u 1 IO OK MW-32 Fluoride 0.1 mg/L l 0.1 OK MW-32 Gross Radium Alpha 0.841 pCi/L l l OK MW-32 Iron 200 ug/L 10 30 OK MW-32 Lead l ug/L u l l OK MW-32 Magnesium 2 mg/L 10 0.5 OK MW-32 Manganese 10 ug/L 5 10 OK MW-32 Mercury 0.5 ug/L u 1 0.5 OK MW-32 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-32 Methylene Chloride 1 ug/L u 1 l OK MW-32 Molybdenum 10 ug/L l 10 OK MW-32 Naphthalene 1 ug/L u 1 I OK MW-32 Nickel 20 ug/L 1 20 OK MW-32 Nitrate + Nitrite as N 0.1 mg/L u l 0.1 OK MW-32 Nitrogen, Ammonia as N 0.2 mg/L 1 0.05 OK MW-32 Potassium 5 mg/L 10 0.5 OK MW-32 Selenium 5 ug/L u l 5 OK MW-32 Silver 10 ug/L u 1 10 OK MW-32 Sodium 5 mg/L 10 0.5 OK MW-32 Sulfate 50 mg/L 50 1 OK MW-32 Tetrahydrofuran l ug/L u 1 l OK MW-32 Thallium 0.5 ug/L u l 0.5 OK MW-32 Tin 100 ug/L u l 100 OK MW-32 Toluene 1 ug/L u 1 l OK MW-32 Uranium 0.5 ug/L l 0.3 OK MW-32 Vanadium 15 ug/L u 1 15 OK MW-32 Xvlenes, total l ug/L u 1 1 OK MW-32 Zinc 10 ug/L 1 10 OK MW-32 Total Dissolved Solids 20 MG/L 1 10 OK MW-35 Acetone 20 ug/L u l 20 OK MW-35 Arsenic 5 ug/L u I 5 OK MW-35 Benzene l ug/L u l 1 OK MW-35 Beryllium 0.5 ug/L u l 0.5 OK G5AQ -I S I R uarter1y amp e eoortm,q, 1m1t ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-35 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-35 Cadmium 0.5 ug/L u 1 0.5 OK MW-35 Calcium 0.2 mg/L 1 0.5 OK MW-35 Carbon Tetrachloride l ug/L u I 1 OK MW-35 Carbonate as C03 1 mg/L u 1 1 OK MW-35 Chloride 5 mg/L 5 1 OK MW-35 Chloroform 1 ug/L u 1 1 OK MW-35 Chloromethane 1 ug/L u 1 1 OK MW-35 Chromium 25 ug/L u 1 25 OK MW-35 Cobalt 10 ug/L u 1 10 OK MW-35 Coooer 10 ug/L u 1 IO OK MW-35 Fluoride 0.1 mg/L 1 0.1 OK MW-35 Gross Radium Alpha 0.756 pCi/L 1 1 OK MW-35 Iron 30 ug/L 1 30 OK MW-35 Lead 1 ug/L u 1 1 OK MW-35 Magnesium 0.2 mg/L 1 0.5 OK MW-35 Manganese 10 ug/L 1 10 OK MW-35 Mercury 0.5 ug/L u 1 0.5 OK MW-35 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-35 Methylene Chloride 1 ug/L u I 1 OK MW-35 Molybdenum 10 ug/L u 1 IO OK MW-35 Naphthalene I ug/L u I I OK MW-35 Nickel 20 ug/L u 1 20 OK MW-35 Nitrate+ Nitrite as N 0.1 mg/L u 1 0.1 OK MW-35 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-35 Potassium 0.5 mg/L I 0.5 OK MW-35 Selenium 5 ug/L 1 5 OK MW-35 Silver 10 ug/L u I IO OK MW-35 Sodium 0.5 mg/L 1 0.5 OK MW-35 Sulfate 50 mg/L 50 1 OK MW-35 Tetrahydrofuran 1 ug/L u 1 1 OK MW-35 Thallium 0.5 ug/L u 1 0.5 OK MW-35 Tin 100 ug/L u 1 100 OK MW-35 Toluene 1 ug/L u 1 1 OK MW-35 Total Dissolved Solids 500 MG/L 1 10 OK MW-35 Uranium 0.5 ug/L 1 0.3 OK MW-35 Vanadium 15 ug/L u 1 15 OK MW-35 Xylenes, total 1 ug/L u 1 1 OK MW-35 Zinc 10 ug/L u 1 10 OK MW-36 Acetone 20 ug/L u 1 20 OK MW-36 Arsenic 5 ug/L u I 5 OK MW-36 Benzene 1 ug/L u 1 1 OK MW-36 Beryllium 0.5 ug/L u l 0.5 OK MW-36 Bicarbonate as CaC03 1 mg/L 1 1 OK MW-36 Cadmium 0.5 ug/L u 1 0.5 OK MW-36 Calcium 0.2 mg/L 1 0.5 OK MW-36 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-36 Carbonate as C03 1 mg/L u 1 1 OK MW-36 Chloride 5 mg/L 5 1 OK MW-36 Chloroform 1 ug/L u 1 1 OK MW-36 Chloromethane 1 ug/L u 1 1 OK MW-36 Chromium 25 ug/L u 1 25 OK MW-36 Cobalt 10 ug/L u 1 IO OK MW-36 Copper 10 ug/L u 1 10 OK G5AQ -IR uarter1y ::>amp e eporung 1m1t ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-36 Fluoride 0.1 mg/L 1 0.1 OK MW-36 Gross Radium Alpha 0.446 pCi/L u 1 1 OK MW-36 Iron 30 ug/L l 30 OK MW-36 Lead 1 ug/L u 1 1 OK MW-36 Magnesium 0.2 mg/L 1 0.5 OK MW-36 Manganese 10 ug/L u I 10 OK MW-36 Mercury 0.5 ug/L u I 0.5 OK MW-36 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-36 Methylene Chloride l ug/L u 1 1 OK MW-36 Molybdenum 10 ug/L u 1 10 OK MW-36 Naphthalene l ug/L u 1 1 OK MW-36 Nickel 20 ug/L u 1 20 OK MW-36 Nitrate + Nitrite as N 0.1 mg/L l 0.1 OK MW-36 Nitrogen, Ammonia as N 0.05 mg/L u l 0.05 OK MW-36 Potassium 0.5 mg/L I 0.5 OK MW-36 Selenium 5 ug/L 1 5 OK MW-36 Silver 10 ug/L u 1 10 OK MW-36 Sodium 2.5 mg/L 5 0.5 OK MW-36 Sulfate 50 mg/L 50 1 OK MW-36 Tetrahydrofuran 1 ug/L u 1 1 OK MW-36 Thallium 0.5 ug/L I 0.5 OK MW-36 Tin 100 ug/L u 1 100 OK MW-36 Toluene l ug/L u I l OK MW-36 Total Dissolved Solids 20 MG/L I 10 OK MW-36 Uranium 0.5 ug/L 1 0.3 OK MW-36 Vanadium 15 ug/L u 1 15 OK MW-36 Xylenes, total 1 ug/L u I 1 OK MW-36 Zinc 10 ug/L u I JO OK MW-37 Acetone 20 ug/L u I 20 OK MW-37 Arsenic 5 ug/L u 1 5 OK MW-37 Benzene l ug/L u 1 I OK MW-37 Beryllium 0.5 ug/L u I 0.5 OK MW-37 Bicarbonate as CaC03 1 mg/L I I OK MW-37 Cadmium 0.5 ug/L u I 0.5 OK MW-37 Calcium l mg/L 5 0.5 OK MW-37 Carbon Tetrachloride I ug/L u I l OK MW-37 Carbonate as C03 I mg/L u l I OK MW-37 Chloride l mg/L l l OK MW-37 Chloroform I ug/L u I l OK MW-37 Chloromethane I ug/L u I l OK MW-37 Chromium 25 ug/L u 1 25 OK MW-37 Cobalt 10 ug/L u I IO OK MW-37 Copper 10 ug/L u I 10 OK MW-37 Fluoride 0.1 mg/L 1 0.1 OK MW-37 Gross Radium Alpha 0.663 pCi/L u 1 1 OK MW-37 Iron 100 ug/L u 5 30 OK MW-37 Lead I ug/L u I I OK MW-37 Magnesium I mg/L 5 0.5 OK MW-37 Manganese IO ug/L u 1 10 OK MW-37 Mercury 0.5 ug/L u 1 0.5 OK MW-37 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-37 Methylene Chloride I ug/L u I 1 OK MW-37 Molybdenum 10 ug/L u I IO OK MW-37 Naphthalene 1 ug/L u 1 1 OK G-5A Quarterly Sample Reporting Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-37 Nickel 20 ug/L u I 20 OK MW-37 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-37 Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-37 Potassium 2.5 mg/L 5 0.5 OK MW-37 Selenium 5 ug/L 1 5 OK MW-37 Silver 10 ug/L u I 10 OK MW-37 Sodium 2.5 mg/L 5 0.5 OK MW-37 Sulfate 100 mg/L 100 I OK MW-37 Tetrahydrofuran 1 ug/L u I I OK MW-37 Thallium 0.2 ug/L l 0.5 OK MW-37 Tin 100 ug/L u 5 100 OK MW-37 Toluene 1 ug/L u 1 1 OK MW-37 Total Dissolved Solids 20 MG/L l 10 OK MW-37 Uranium 0.3 ug/L 1 0.3 OK MW-37 Vanadium 15 ug/L u l 15 OK MW-37 Xvlenes, total 1 ug/L u I 1 OK MW-37 Zinc 10 ug/L 1 10 OK MW-38 Acetone 20 ug/L u 1 20 OK MW-38 Arsenic 5 ug/L u 1 5 OK MW-38 Benzene 1 ug/L u l 1 OK MW-38 Beryllium 0.5 ug/L u 1 0.5 OK MW-38 Bicarbonate as CaC03 I mg/L 1 1 OK MW-38 Cadmium 0.5 ug/L u I 0.5 OK MW-38 Calcium 0.2 mg/L I 0.5 OK MW-38 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-38 Carbonate as C03 1 mg/L u 1 1 OK MW-38 Chloride 20 mg/L 20 1 OK MW-38 Chloroform 1 ug/L u I 1 OK MW-38 Chloromethane I ug/L u I 1 OK MW-38 Chromium 25 ug/L u I 25 OK MW-38 Cobalt 10 ug/L u I 10 OK MW-38 Copper 10 ug/L u I 10 OK MW-38 Fluoride 0.1 mg/L 1 0.1 OK MW-38 Gross Radium Alpha 0.502 pCi/L u 1 1 OK MW-38 Iron 30 ug/L u 1 30 OK MW-38 Lead I ug/L u I 1 OK MW-38 Magnesium 0.2 mg/L 1 0.5 OK MW-38 Manganese 10 ug/L u 1 10 OK MW-38 Mercury 0.5 ug/L u 1 0.5 OK MW-38 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-38 Methylene Chloride 1 ug/L u 1 1 OK MW-38 Molybdenum 10 ug/L u I 10 OK MW-38 Naphthalene I ug/L u I I OK MW-38 Nickel 20 ug/L u 1 20 OK MW-38 Nitrate + Nitrite as N 0.1 mg/L I 0.1 OK MW-38 Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-38 Potassium 0.5 mg/L 1 0.5 OK MW-38 Selenium 5 ug/L I 5 OK MW-38 Silver 10 ug/L u 1 JO OK MW-38 Sodium 0.5 mg/L I 0.5 OK MW-38 Sulfate 20 mg/L 20 I OK MW-38 Tetrahydrofuran 1 ug/L u 1 I OK MW-38 Thallium 0.2 ug/L u 1 0.5 OK MW-38 Tin 100 ug/L u 1 100 OK G 5AQ -I S l R oaner1y amp e eporting 1m1t ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analvte Limit Units Qualifier Factor Limit Check MW-38 Toluene 1 ug/L u 1 1 OK MW-38 Total Dissolved Solids 20 MG/L 1 10 OK MW-38 Uranium 0.3 ug/L 1 0.3 OK MW-38 Vanadium 15 ug/L u 1 15 OK MW-38 Xylenes, total 1 ug/L u 1 1 OK MW-38 Zinc 10 ug/L u 1 10 OK MW-39 Acetone 20 ug/L u 1 20 OK MW-39 Arsenic 5 ug/L u 1 5 OK MW-39 Benzene 1 ug/L u I 1 OK MW-39 Beryllium 0.5 ug/L 1 0.5 OK MW-39 Bicarbonate as CaC03 I mg/L u 1 1 OK MW-39 Cadmium 0.5 ug/L 1 0.5 OK MW-39 Calcium 0.2 mg/L 1 0.5 OK MW-39 Carbon Tetrachloride I ug/L u I 1 OK MW-39 Carbonate as C03 I mg/L u 1 1 OK MW-39 Chloride 5 mg/L 5 1 OK MW-39 Chloroform I ug/L u I l OK MW-39 Chloromethane 1 ug/L u 1 I OK MW-39 Chromium 25 ug/L u I 25 OK MW-39 Cobalt 10 ug/L I 10 OK MW-39 Copper 10 ug/L 1 10 OK MW-39 Fluoride 0.5 mg/L 5 0.1 OK MW-39 Gross Radium Alpha 0.504 pCi/L l 1 OK MW-39 Iron 30 ug/L 1 30 OK MW-39 Lead 1 ug/L u 1 I OK MW-39 Magnesium 0.2 mg/L l 0.5 OK MW-39 Manganese 10 ug/L 1 10 OK MW-39 Mercury 0.5 ug/L u I 0.5 OK MW-39 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-39 Methylene Chloride 1 ug/L u 1 1 OK MW-39 Molybdenum 10 ug/L u 1 10 OK MW-39 Naphthalene 1 ug/L u 1 1 OK MW-39 Nickel 20 ug/L I 20 OK MW-39 Nitrate+ Nitrite as N 0.1 mg/L 1 0.1 OK MW-39 Nitrogen, Ammonia as N 0.05 mg/L I 0.05 OK MW-39 Potassium 0.5 mg/L 1 0.5 OK MW-39 Selenium 5 ug/L I 5 OK MW-39 Silver 10 ug/L u 1 10 OK MW-39 Sodium 2.5 mg/L 5 0.5 OK MW-39 Sulfate 50 mg/L 50 1 OK MW-39 Tetrahydrofuran 1 ug/L u 1 1 OK MW-39 Thallium 0.5 ug/L I 0.5 OK MW-39 Tin 100 ug/L u 1 100 OK MW-39 Toluene 1 ug/L u 1 1 OK MW-39 Total Dissolved Solids 20 MG/L 1 10 OK MW-39 Uranium 0.5 ug/L 1 0.3 OK MW-39 Vanadium 15 ug/L u 1 15 OK MW-39 X vlenes, total 1 ug/L u 1 1 OK MW-39 Zinc IO ug/L 1 10 OK MW-40 Acetone 20 ug/L u 1 20 OK MW-40 Arsenic 5 ug/L u 1 5 OK MW-40 Benzene 1 ug/L u 1 1 OK MW-40 Beryllium 0.5 ug/L u 1 0.5 OK MW-40 Bicarbonate as CaC03 1 mg/L 1 1 OK G5AQ -IR uarter1y ~amp e eporting 1m1t ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-40 Cadmium 0.5 ug/L u 1 0.5 OK MW-40 Calcium 0.2 mg/L I 0.5 OK MW-40 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-40 Carbonate as C03 1 mg/L u I 1 OK MW-40 Chloride 5 mg/L 5 l OK MW-40 Chloroform 1 ug/L u I 1 OK MW-40 Chloromethane 1 ug/L u I 1 OK MW-40 Chromium 25 ug/L u I 25 OK MW-40 Cobalt 10 ug/L u 1 10 OK MW-40 Copper 10 ug/L u I 10 OK MW-40 Fluoride 0.5 mg/L 5 0.1 OK MW-40 Gross Radium Alpha 0.684 pCi/L u 1 1 OK MW-40 Iron 30 ug/L u 1 30 OK MW-40 Lead 1 ug/L u 1 1 OK MW-40 Magnesium 0.2 mg/L 1 0.5 OK MW-40 Manganese 10 ug/L I 10 OK MW-40 Mercury 0.5 ug/L u I 0.5 OK MW-40 Methyl Ethyl Ketone 20 ug/L u l 20 OK MW-40 Methylene Chloride l ug/L u 1 1 OK MW-40 Molybdenum 10 ug/L u 1 10 OK MW-40 Naphthalene 1 ug/L u 1 1 OK MW-40 Nickel 20 ug/L u 1 20 OK MW-40 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-40 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-40 Potassium 0.5 mg/L 1 0.5 OK MW-40 Selenium 5 ug/L 1 5 OK MW-40 Silver IO ug/L u 1 10 OK MW-40 Sodium 0.5 mg/L 1 0.5 OK MW-40 Sulfate 50 mg/L 50 1 OK MW-40 Tetrahydrofuran I ug/L u 1 1 OK MW-40 Thallium 0.5 ug/L u 1 0.5 OK MW-40 Tin 100 ug/L u 1 100 OK MW-40 Toluene 1 ug/L u l I OK MW-40 Total Dissolved Solids 20 MG/L I 10 OK MW-40 Uranium 2.5 ug/L 5 0.3 bK MW-40 Vanadium 15 ug/L u 1 15 OK MW-40 Xylenes, total 1 ug/L u 1 1 OK MW-40 Zinc 10 ug/L u 1 10 OK MW-65 Acetone 20 ug/L u 1 20 OK MW-65 Arsenic 5 ug/L u 1 5 OK MW-65 Benzene 1 ug/L u l 1 OK MW-65 Beryllium 0.5 ug/L u l 0.5 OK MW-65 Bicarbonate as CaC03 1 mg/L 1 l OK MW-65 Cadmium 0.5 ug/L u 1 0.5 OK MW-65 Calcium 0.2 mg/L 1 0.5 OK MW-65 Carbon Tetrachloride 1 ug/L u 1 I OK MW-65 Carbonate as C03 1 mg/L u 1 1 OK MW-65 Chloride 5 mg/L 5 1 OK MW-65 Chloroform 1 ug/L u 1 1 OK MW-65 Chloromethane I ug/L u 1 1 OK MW-65 Chromium 25 ug/L u 1 25 OK MW-65 Cobalt 10 ug/L u l 10 OK MW-65 Coooer 10 ug/L u 1 10 OK MW-65 Fluoride 0.5 mg/L 5 0.1 OK G 5AQ -I S I R uarter ,y amp e eportrng 1m1t ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analvte Limit Units Qualifier Factor Limit Check MW-65 Gross Radium Alpha 0.815 pCi/L u 1 1 OK MW-65 Iron 30 ug/L 1 30 OK MW-65 Lead 1 ug/L u 1 1 OK MW-65 Magnesium 0.2 mg/L 1 0.5 OK MW-65 Manganese 10 ug/L 5 10 OK MW-65 Mercury 0.5 ug/L u 1 0.5 OK MW-65 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-65 Methylene Chloride 1 ug/L u 1 1 OK MW-65 Molybdenum 10 ug/L u 1 10 OK MW-65 Naphthalene 1 ug/L u I I OK MW-65 Nickel 20 ug/L u 1 20 OK MW-65 Nitrate + Nitrite as N 0.1 mg/L u 1 0.1 OK MW-65 Nitrogen, Ammonia as N 0.2 mg/L 1 0.05 OK MW-65 Potassium 0.5 mg/L 1 0.5 OK MW-65 Selenium 5 ug/L u 1 5 OK MW-65 Silver 10 ug/L u 1 10 OK MW-65 Sodium 0.5 mg/L 1 0.5 OK MW-65 Sulfate 50 mg/L 50 I OK MW-65 Tetrahydrofuran 1 ug/L u 1 1 OK MW-65 Thallium 0.5 ug/L u 1 0.5 OK MW-65 Tin 100 ug/L u 1 100 OK MW-65 Toluene 1 ug/L u 1 1 OK MW-65 Total Dissolved Solids 20 MG/L 1 10 OK MW-65 Uranium 0.5 ug/L 1 0.3 OK MW-65 Vanadium 15 ug/L u 1 15 OK MW-65 Xylenes, total 1 ug/L u 1 1 OK MW-65 Zinc 10 ug/L u 1 10 OK MW-70 Acetone 20 ug/L u 1 20 OK MW-70 Arsenic 5 ug/L u 1 5 OK MW-70 Benzene 1 ug/L u 1 1 OK MW-70 Beryllium 0.5 ug/L u 1 0.5 OK MW-70 Bicarbonate as CaC03 I mg/L 1 1 OK MW-70 Cadmium 0.5 ug/L u 1 0.5 OK MW-70 Calcium 0.2 mg/L 1 0.5 OK MW-70 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-70 Carbonate as C03 1 mg/L u 1 1 OK MW-70 Chloride 5 mg/L 5 1 OK MW-70 Chloroform 1 ug/L u 1 1 OK MW-70 Chloromethane 1 ug/L u 1 1 OK MW-70 Chromium 25 ug/L u 1 25 OK MW-70 Cobalt 10 ug/L u 1 10 OK MW-70 Coooer 10 ug/L u 1 10 OK MW-70 Fluoride 0.1 mg/L 1 0.1 OK MW-70 Gross Radium Alpha 0.673 pCi/L u 1 1 OK MW-70 Iron 30 ug/L u 1 30 OK MW-70 Lead 1 ug/L u 1 1 OK MW-70 Magnesium 0.2 mg/L 1 0.5 OK MW-70 Manganese 10 ug/L u 1 10 OK MW-70 Mercury 0.5 ug/L u 1 0.5 OK MW-70 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-70 Methylene Chloride 1 ug/L u 1 1 OK MW-70 Molybdenum 10 ug/L u 1 10 OK MW-70 Naphthalene 1 ug/L u 1 1 OK MW-70 Nickel 20 ug/L u 1 20 OK G5AQ -uarteriy amp e I S I R eport-ing 1m1t ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analvte Limit Units Qualifier Factor Limit Check MW-70 Nitrate+ Nitrite as N 0.1 mg/L 1 0.1 OK MW-70 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-70 Potassium 0.5 mg/L 1 0.5 OK MW-70 Selenium 5 ug/L 1 5 OK MW-70 Silver 10 ug/L u 1 10 OK MW-70 Sodium 2.5 mg/L 5 0.5 OK MW-70 Sulfate 50 mg/L 50 1 OK MW-70 Tetrahydrofuran 1 ug/L u 1 1 OK MW-70 Thallium 0.5 ug/L 1 0.5 OK MW-70 Tin 100 ug/L u 1 100 OK MW-70 Toluene 1 ug/L u 1 1 OK MW-70 Total Dissolved Solids 20 MG/L 1 10 OK MW-70 Uranium 0.5 ug/L 1 0.3 OK MW-70 Vanadium 15 ug/L u 1 15 OK MW-70 Xylenes, total 1 ug/L u 1 1 OK MW-70 Zinc 10 ug/L u 1 10 OK TW4-24 Acetone 20 ug/L u 1 20 OK TW4-24 Arsenic 5 ug/L u 1 5 OK TW4-24 Benzene 1 ug/L u 1 1 OK TW4-24 Beryllium 0.5 ug/L u 1 0.5 OK TW4-24 Bicarbonate as CaC03 1 mg/L 1 1 OK TW4-24 Cadmium 0.5 ug/L 1 0.5 OK TW4-24 Calcium 0.4 mg/L 2 0.5 OK TW4-24 Carbon Tetrachloride 1 ug/L u 1 1 OK TW4-24 Carbonate as C03 1 mg/L u 1 1 OK TW4-24 Chloride 100 mg/L 100 1 OK TW4-24 Chloroform 1 ug/L 1 1 OK TW4-24 Chloromethane 1 ug/L u 1 1 OK TW4-24 Chromium 25 ug/L u 1 25 OK TW4-24 Cobalt 10 ug/L u 1 10 OK TW4-24 Copper 10 ug/L u 1 10 OK TW4-24 Fluoride 0.1 mg/L 1 0.1 OK TW4-24 Gross Radium Alpha 0.762 pCi/L u 1 1 OK TW4-24 Iron 40 ug/L u 2 30 OK TW4-24 Lead 1 ug/L u 1 1 OK TW4-24 Magnesium 0.4 mg/L 2 0.5 OK TW4-24 Manganese 10 ug/L 1 10 OK TW4-24 Mercury 0.5 ug/L u 1 0.5 OK TW4-24 Methyl Ethyl Ketone 20 ug/L u 1 20 OK TW4-24 Methylene Chloride 1 ug/L u 1 1 OK TW4-24 Molybdenum 10 ug/L 1 10 OK TW4-24 Naphthalene 1 ug/L u 1 1 OK TW4-24 Nickel 20 ug/L u 1 20 OK TW4-24 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK TW4-24 Nitrogen, Ammonia as N 1.2 mg/L 25 0.05 OK TW4-24 Potassium 1 mg/L 2 0.5 OK TW4-24 Selenium 5 ug/L 1 5 OK TW4-24 Silver 10 ug/L u 1 10 OK TW4-24 Sodium 1 mg/L 2 0.5 OK TW4-24 Sulfate 100 mg/L 100 1 OK TW4-24 Tetrahydrofuran 1 ug/L u 1 1 OK TW4-24 Thallium 0.5 ug/L 1 0.5 OK TW4-24 Tin 100 ug/L u 2 100 OK TW4-24 Toluene 1 ug/L u 1 1 OK G5AQ -ua1terly s ample R eport1ng mut ec L .. Ch k Lab Required Rep@rting. Dill.Ili on Reporcihg RL Location Anal¥te Limit UniLS Qualifier Fael<)r Limit ChecR TW4-24 Total Dissolved Solids 20 MG/L 1 10 OK TW4-24 Uranium 0.5 ug/L 1 0.3 OK TW4-24 Vanadium 15 ug/L u 1 15 OK TW4-24 Xylenes, total 1 ug/L u 1 I OK TW4-24 Zinc 10 ug/L u 1 10 OK G5BA -cce erate dS I R amp e eporung 1m1t ec L' . Ch k Lab Required Reporting Dilution Reporting Location Analyte Limit Units Qualifier Factor Limit RLCheck Trip Blank Chloroform 1 ug/L u 1 1 OK Trip Blank Toluene 1 ug/L u 1 I OK Trip Blank Tetrahydrofurau 1 ug/L u 1 1 OK Trip Blank Xylenes, total 1 ug/L u 1 1 OK Trip Blank Carbon Tetrachloride 1 ug/L u 1 1 OK Trip Blank Acetone 20 ug/L u 1 20 OK Trip Blank Chloroform 1 ug/L u 1 1 OK Trip Blank Benzene 1 ug/L u 1 1 OK Trip Blank Chloromethane 1 ug/L u 1 1 OK Trip Blank Methylene Chloride 1 ug/L u 1 1 OK Trip Blank Methyl Ethyl Ketone 20 ug/L u 1 20 OK Trip Blank Naphthalene 1 ug/L u 1 I OK MW-11 Sulfate 20 mg/L 20 1 OK MW-11 Chloride 1 mg/L 1 1 OK MW-11 Manganese 10 ug/L 1 10 OK MW-11 Nitrate+ Nitrite as N 0.1 mg/L 1 0.1 OK MW-11 Total Dissolved Solids 20 MG/L 2 10 OK MW-11 Sulfate 10 mg/L 10 1 OK MW-11 Chloride 1 mg/L 1 1 OK MW-11 Manganese 10 ug/L 1 10 OK MW-11 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-11 Total Dissolved Solids 20 MG/L 2 10 OK MW-25 Total Dissolved Solids 20 MG/L 2 10 OK MW-25 Total Dissolved Solids 20 MG/L 2 10 OK MW-26 Chloride 10 mg/L 10 1 OK MW-26 Chloroform 50 ug/L 50 1 OK MW-26 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-26 Total Dissolved Solids 20 MG/L 2 10 OK MW-26 Toluene 1 ug/L u 1 1 OK MW-26 Tetrahydrofuran 1 ug/L u 1 I OK MW-26 Xylenes, total 1 ug/L u 1 I OK MW-26 Chloride I mg/L 1 1 OK MW-26 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-26 Acetone 20 ug/L u 1 20 OK MW-26 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-26 Total Dissolved Solids 20 MG/L 2 10 OK MW-26 Chloroform 100 ug/L MS-High 100 1 OK MW-26 Benzene 1 ug/L u 1 1 OK MW-26 Chloromethane 1 ug/L u 1 1 OK MW-26 Methylene Chloride I ug/L u 1 1 OK MW-26 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-26 Naphthalene I ug/L u 1 1 OK MW-30 Chloride 10 mg/L 10 1 OK MW-30 Uranium 0.3 ug/L 1 0.3 OK MW-30 Selenium 5 ug/L 1 5 OK MW-30 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-30 Total Dissolved Solids 20 MG/L 2 IO OK MW-30 Chloride IO mg/L 10 1 OK MW-30 Uranium 0.3 ug/L l 0.3 OK MW-30 Selenium 5 ug/L 1 5 OK MW-30 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-30 Total Dissolved Solids 20 MG/L 2 10 OK MW-31 Sulfate 20 mg/L 20 1 OK MW-31 Chloride 10 mg/L 10 I OK G5BA -cce erate dS I R ampe eporLing L" . Ch k 1m1t ec Lab Required Reporting Dilution Reporting Location Analyte Limit Units Qualifier Factor Limit RLCheck MW-31 Uranium 0.3 ug/L 1 0.3 OK MW-31 Nitrate+ Nitrite as N 0.5 mg/L 5 0.1 OK MW-31 Total Dissolved Solids 20 MG/L 2 IO OK MW-31 Sulfate 20 mg/L 20 l OK MW-31 Chloride IO mg/L 10 I OK MW-31 Uranium 0.3 ug/L I 0.3 OK MW-31 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-31 Total Dissolved Solids 20 MG/L 2 IO OK MW-65 Chloride 5 mg/L 5 1 OK MW-65 Uranium 0.3 ug/L I 0.3 OK MW-65 Selenium 5 ug/L 1 5 OK MW-65 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-65 Total Dissolved Solids 20 MG/L 2 10 OK MW-65 Total Dissolved Solids 20 MG/L 2 10 OK G-6A: Quarterly, ample Trip Blank Evaluation Lab Report Constituent Result 2-Butanone ND Acetone ND Benzene ND Carbon Tetrachloride ND Chloroform ND CTF22D1197 Chloromethane ND Methylene Chloride ND Naphthalene ND Tetrahydrofuran ND Toluene ND Xvlenes, Total ND 2-Butanone ND Acetone ND Benzene ND Carbon Tetrachloride ND Chloroform ND CTF 22Dl691 Chloromethane ND Methylene Chloride ND Naphthalene ND Tetrahydrofuran ND Toluene ND Xylenes, Total ND 2-Butanone ND Acetone ND Benzene ND Carbon Tetrachloride ND Chloroform ND CTF 22D2139 Chloromethane ND Methavlene Chloride ND Naphthalene ND Tetrahydrofuran ND Toluene ND Xylenes, Total ND 2-Butanone ND Acetone ND Benzene ND Carbon Tetrachloride ND Chloroform ND CTF 22El503 Chloromethane ND Methaylene Chloride ND Naphthalene ND Tetrahydrofuran ND Toluene ND Xvlenes, Total ND G-6B: Accelerated Sample Trip Blank Evaluation All trip blanks for the Accelerated samples were non detect. Blank Sample Date Laboratory CTF 22E0524 -May 5/4/2022 CTF CTF 22F0888 -June 6/7/2022 CTF G -7A: A Q /QC Evaluation for Quarterly Sam1Jle Duolicates Constituent MW-29 MW-65 %RPO 4/14/22 4/14/22 Ammonia (as N) (mg/L) 0.4 0.6 40.00 Bicarbonate as CaC03 (mg/L) 307 307 0.00 Calcium (mg/L) 410 415 1.21 Chloride (mwl) 34.2 34.4 0.58 Fluoride (mg/L) 0.8 0.5 46.15 Tron (m_g/L) 1.05 1.09 3.74 Magnesium (mg/L) 199 202 1.50 Manganese (1112/L) 5.03 5.02 0.20 Nitrate + Nitrite (as N) (mg/L) 0.1 <0.1 NIA Potassium (mg/L) 15.2 15.7 3.24 Sodium (mg/L) 383 395 3.08 Sulfate (mg/L) 2550 2550 0.00 TDS (mg/L) 4000 4070 1.73 Uranium (mg/L) 0.0157 0.0155 1.28 Constituent MW-36 MW-70 %RPO 4/21/22 4/21/22 Bicarbonate as HC03 273 252 8.00 Calcium (mg/L) 354 359 1.40 Chloride (m.WL) 54.6 55.0 0.73 Fluoride (mg/L) 0.3 0.3 0.00 Iron 0.07 <0.03 NIA Magnesium (mg/L) 121 122 0.82 Nitrate + Nitrite (as N) 0.2 0.3 40.00 Potassium (mg/L) 8.8 8.9 1.13 Selenium (mg/L) 0.256 0.263 2.70 Sodium (mg/L) 674 680 0.89 Sulfate (mg/L) 2560 2560 0.00 IDS (mg/L) 3890 3540 9.42 Thallium 0.0006 0.0006 0.00 Uranium (mg/L) 0.0228 0.0232 1.74 Per the approved QAP, an RPD greater than 20% is acceptable if the reported results are less than 5 times the RL. These results are provided for information only. NIA -The duplicate test was not performed hecause both results were not greater than the RL. G 7B QA/QC E l f A -va uat10n or cce erate d I D r ~amp e up 1cates MW-30 MW-65 Constitu~t 5/4/22 5/4/22 %RPD* Nitrate + Nitrite (as N) (mJ?,/L) 15 15 0.00 Selenium (mg/L) 0.0694 0.0690 0.58 Uranium (mg/L) 0.0101 0.0101 0.00 Chloride (rng/L) 195 202 3.53 TDS(mg/L) 1640 1600 2.47 MW-25 MW-65 Constituent 6nt22 617/22 %RPO Total Dissolved Solids (mg/L) 2730 2540 7.21 G-8A: Radiologies Counting Error Gross Alpha Counting Gross Alpha minus Rn and U Error :S Within Well Sample Date minusRn&U Precision ( +/-) 20% GWCL GWCL? MW-01 04/14/22 l.OOU 0.240 NC - MW-02 04/12/22 l.OOU 0.249 NC 3.2 NC MW-03A 04/27/22 l.OOU 0.288 NC 7.5 NC MW-05 04/18/22 l.OOU 0.139 NC 3.75 NC MW-11 04/18/22 l.OOU 0.211 NC 3.75 NC MW-12 04/19/22 l.OOU 0.154 NC 7.5 NC MW-14 04/18/22 l.OOU 0.126 NC 7.5 NC MW-15 04/19/22 l.OOU 0.134 NC 7.5 NC MW-17 04/18/22 l.OOU 0.182 NC 2.8 NC MW-18 04/13/22 l.OOU 0.219 NC - MW-19 04/13/22 l.OOU 0.283 NC - MW-20 05/17/22 l.OOU 0.160 NC - MW-22 04/25/22 2.05 0.439 N - MW-23 04/27/22 l.OOU 0.247 NC 2.86 NC MW-24 04/27/22 2.28 0.432 y 7.5 NC MW-24A 04/27/22 3.10 0.493 y - MW-25 04/12/22 l.OOU 0.210 NC 2.86 NIA MW-26 Resample 04/27/22 1.00 U 0.308 NC 4.69 NC MW-27 04/12/22 1.18 0.374 N 4.69 y MW-28 04/19/22 l.OOU 0.280 NC 2.42 NC MW-29 04/14/22 l.OOU 0.219 NC 2.42 NC MW-30 04/20/22 l.OOU 0.180 NC 3.75 NC MW-31 04/11/22 l.OOU 0.294 NC 7.5 NC MW-32 04/11/22 1.82 0.445 N 3.33 y MW-35 04/12/22 3.75 0.560 y 7.5 NIA MW-36 04/21/22 l.OOU 0.231 NC 7.5 NC MW-37 05/17/22 l.OOU 0.290 NC 4.2 NC MW-38 04/27/22 l.OOU 0.223 NC - MW-39 04/20/22 1.36 0.299 N - MW-40 04/19/22 l.OOU 0.274 NC - TW4-24 04/27/22 l.OOU 0.278 NC - MW-65 04/14/22 l.OOU 0.197 NC 2.42 NC MW-70 4/21/2022 l.OOU 0.262 NC 7.5 NC NIA= the counting error is less than 20% of the activity as required by the GWDP and/or the value is above the GWCL and this check column is not applicable. NC= Not calculated. The sample results are nondetect and the check is not applicable. G-8B: Radiologies Counting Error for Accelerated Samples There are no accelerated samples collected for Gross Alpha. G-9A: Quarterly Sample Laboratory Matrix QC Mt· Sik ~R C a nx p e o ecovery om 1>anson Lab Report Well Analyte MS %REC MSD%REC REC Range 22Dl 197 MW-31 Calcium* NC NC 70-130 MW-65 (Duplicate of MW 22Dl 197 29) Calcium* NC NC 70-130 MW-65 (Duplicate of MW 22Dl 197 29) Manganese* NC NC 70-130 22Dl 197 NA Fluoride 52.3 64.2 80-120 22Dl 197 MW-31 Nitrate 78.1 109 80-120 22Dl 197 MW-31 Tetrahydrofuran 133 118 70-130 22D1691 MW-5 Calcium* NC NC 70-130 22D169l MW-5 Sodium* NC NC 70-130 22D1691 MW-11 Sulfate 71.5 62.3 80-120 22D1691 MW-14 Sulfate 46.0 29 80-120 22D169l NA Nitrate 122 121 80-120 22D2139 NA Calcium* NC NC 70-130 22D2139 NA Sodium* NC NC 70-130 22D2139 MW-22 Calcium* NC NC 70-130 22D2139 MW-22 Iron 418 441 70-130 22D2139 MW-22 Magnesium* NC NC 70-130 22D2139 MW-22 Potassium 431 428 70-130 22D2139 MW-22 Sodium* NC NC 70-130 22D2139 MW-22 Tin 404 401 70-130 22D2139 NA Silver -0.667 ** 70-130 22D2139 MW-22 Cobalt* NC NC 70-130 22D2139 MW-22 Manganese* NC NC 70-130 22D2139 MW-22 Molybdenum* NC NC 70-130 22D2139 MW-22 Nickel* NC NC 70-130 22D2139 MW-22 Zinc* NC NC 70-130 22D2139 MW-22 Fluoride 52.3 62.4 80-120 22D2139 MW-22 Sulfate 52.3 NC 70-130 22E1503 MW-20 Sodium* NC NC 70-130 22E1503 NA Chloride* NC NC 80-120 22El503 NA Fluoride 19.5 23.6 80-120 22E1503 MW-20 Nitrate 76.5 96.9 80-120 22El503 MW-20 Acetone 69.2 69.3 70-130 22E1503 MW-20 Chloromethane 67.3 68.1 70-130 576962 MW-31 Gross Alpha 76.6 70.5 75-125 578558 and 580437 MW-22 Gross Alpha 51.3 58.8 75-125 * Recovery was not calculated as the analyte level in the sample was greater than 4 times the spike amount. NA -QC was not performed on an EFRI sample. RPD RPD Range NC 20 NC 20 NC 20 17.4 20 1.66 20 12.1 20 NC 20 NC 20 2.76 20 3.3 20 0.227 20 NC 20 NC 20 NC 20 4.79 20 NC 20 0.348 20 NC 20 0.761 20 ** ** NC 20 NC 20 NC 20 NC 20 NC 20 17.4 20 NC 20 NC 20 NC 20 19 20 2.26 20 0.0867 20 1.18 20 7.88 20 10.2 20 ** CTF routine QC does not include a MDS for metals analyzed by 200.8. Precision is determined by other QC samples as allowable by the analytical method. G-9A: Quarterly Sample Laboratory Matrix QC Method Blank Detections All Method Blanks for the quarter were non-detect. Lb t C t IS a ora ory on ro amp1e Lab Report Analyte LCS %REC REC Ranee 22El503 Iron 128 85-115 22E1503 Acetone 68.6 70-130 22E1503 Tetrahydrofuran 131.0 70-130 L b a oratory D r up11cate 0 ecovery C ompanson Sample R~ult Lab RPD Lab Report Wen Analyte (mg/L) Duplicate RPO% Range 22D2139 MW-22 Total Dissolved Solids* NC NC NC 10 * Recovery was not calculated due to the high analyte level in the sample. G-9B: Accelerated Laboratory Matrix QC Matrix Spike % Reco,•ery C -- RPDRange Lab Report Well Analyte MS %REC MSD %REC REC Range RPO% % 22E0524 -May Monthly MW-II Sulfate* NC NC 80-120 NC 20 22E0524 -May Monthly MW-31 Sulfate* NC NC 80-120 NC 20 22E0524 -May Monthly NA Chloride 66.8 97.3 80-120 4.86 20 22E0524 -May MonLhly MW-30 Nitrate 88.2 76.4 80-120 0.726 20 22E0524 -May Monthly MW-26 Chloroform* NC NC 70-130 NC 20 22F0888 -June Monthly MW-11 Chloride 64.1 66.7 80-120 0.549 20 22F0888 -June Monthly MW-11 Sulfate* NC NC 80-120 NC 20 22F0888 -June Monthly MW-26 Sulfate* NC NC 80-120 NC 20 22F0888 -June Monthly MW-11 Nitrate 79.2 95.1 80-120 5.79 20 22F0888 -June Monthly MW-26 Chloroform* NC NC 70-130 NC 20 22F0888 -June Monthly MW-26 Chloromethane 62.1 73.8 70-130 17.2 20 * Recovery was not calculated as the analyte level in the sample was greater than 4 times the spike amount Laboratory Control Sample Lab Report Analyte LCS %REC REC Range 22E0524 MEK 137 70-130 Method Blank Detections All Method Blanks for the quarter were non-detect. TabH Kriged Current Quarterly Groundwater Contour Map @ TW4-43 ~5523 TWN-20 1]5564 TW4-42 ¢ 5525 estimated dry area temporary perched monitoring well installed September, 2021 showing elevation in feet amsl temporary perched nitrate monitoring well installed April, 2021 showing elevation in feet amsl temporary perched monitoring well installed April, 2019 showing elevation in feet amsl MW-38 perched monitoring well "¢-5463 installed February, 2018 showing elevation in feet amsl M;-~504 perched monitoring well showing elevation in feet amsl . TW4-12 . . I 0 5568 temporary perched monitoring well showing elevation in feet amsl TWN-7 . . . A.5569 temporary perched nitrate monitoring V well showing elevation in feet amsl PIEZ-1 perched piezometer showing ~ 5588 elevation in feet amsl RUIN SPRING o 5380 seep or spring showing elevation in feet amsl NOTES: MW-4, MW-26, TW4-1, TW4-2, TW4-4, TW4-11, TW4-19, TW4-21, TW4-37, TW4-39, TW4-40 and TW4-41 are chloroform pumping wells; TW4-22, TW4-24, TW4-25 and TWN-2 are nitrate pumping wells;~4-1, TW4-2 and TW4-11 water levels are below th~ ba~e_()f the Burro Canyon Formation HYDRO GEO CHEM,INC. KRIGED 2nd QUARTER, 2022 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE H:/718000/aug22/WUUwl0622.srf FIGURE H-1 Tab I Groundwater Time Concentration Plots B INTERA Time concentration plots for MW-01 Chloride in MW-01 Sample Date Fluoride in MW-01 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values 5000 4500 4000 3500 ::;-3000 'iio E '; 2500 ~ ~ 2000 1500 1000 500 0 • ti -- I B INTERA Time concentration plots for MW-01 --. I Sulfate in MW-01 ' -..... ---------- Sample Date Uranium in MW-01 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 -.A..&. ....... -.. • Detected Values Non-Detected Values Time concentration plots for MW-02 Chloride in MW-02 Sample Date Fluoride in MW-02 ::, ~ .§. 0.5 ~----------------------------------1 a, "O -~ 0.4 -HcN----------------1--1-------------1 :::, ;:;: 0.3 B INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-02 Sulfate in MW-02 2500 ~----------------------------- 500 ------------------------------------1 0 • r;"°' 0 14 ::i" 12 } E 10 :::, 'i: .. :) 8 '>:~ ..,-s ~2¥e lN I ERA ~"°' 'I"~ !>,"' '?J'b r;:,"> s:,'b ,; ',e,~ ~'I>"( ,_ef') <:;f Sample Date Uranium in MW-02 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 .P ~o ..:'Y ..,-s • ~;\,"' 'l"q Detected Values Non-Detected Values Time concentration plots for MW-03A Chloride in MW-03A Sample Date Fluoride in MW-03A ~ ] 1 -1---;H---e-----.~-----31iic::,~=-------::1111~--~,--JI----J~l-l Cl/ "'O ·~ 0.8 -t--l+-----------------------1-J-----l-l ::, ii: l!IINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-03A Sulfate in MW-03A 4500 4000 3500 3000 ::; } 2500 QI .. :Ill 2000 :::, <II 1500 1000 500 0 ~<, ~ f:l°' ..,_.<1' ~"'"' ~,§ Sample Date Uranium in MW-03A -25 tt--1~----------------:=-----------------1 1 § 20 tt-~----t---..--.;;;;;;;;il!C"""r--\Jr-"°""-;~.--.----------::::;;;a;.-----;r....::::1 ·c ~ ::::, 15 -i....-t-------------------------------1 BINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-05 Chloride in MW-OS 140 120 • 100 :::i' ....... 80 '"' g Cl ~ ..Q 60 .c u 40 0 +-----,----,------,----,------~-----.---~------1 :::i' ....... '"' 1 g Cl "'C -~ 0.8 :I ;:;: 111!:'\;INTERA Sample Date Fluoride in MW-OS Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values Time concentration plots for MW-05 9000 8000 7000 6000 i 5000 .21 ~ 4000 ::, "' 3000 2000 1000 0 160 140 120 _ 100 ... ....... 00 -== E 80 ::, ·2 "' ... ::::, 60 40 20 0 ' ·-I. L ' -- l!IINTERA - Sulfate in MW-OS i --.. -- Sample Date Uranium in MW-OS --· -• ; Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 ~----..~-....... • A ....... • Detected Values Non-Detected Values -50 ~ -5. a, 40 -0 ·c:: 0 :c u 30 0.8 0.7 0.6 -0.5 ..... ~ -5. QJ 0.4 -0 ·.::: 0 :::, ii: 0.3 0.2 0.1 0 ~ ~'b ~'Ii ,;. c,fbQ BINTERA Time concentration plots for MW-11 Chloride in MW-11 Sample Date Fluoride in MW-11 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values 4.5 4 • 3.5 3 ::;-"iio .=: 2.5 E :::, 'i: 2 "' .. :) 1.5 1 0.5 0 :>, ~ :>..'b .,e-~ ~'b ~islNTERA Time concentration plots for MW-11 Sulfate in MW-11 Sample Date Uranium in MW-11 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-12 Chloride in MW-12 160 ..-----------------------------~ 140 +----t------------------------------1 120 ·t----a----------------------------l _100 +-----------------------------------1 ..I 'tio .§. ~ 80 'l'---t•---------------------------1 ·.: 0 a 60 20 ;-------------------------------1 0 +----.-----.----..-----,----,---~~--~--~---I 0.4 0.35 0.3 _ 0.25 ..I 'tio .§. GI 0.2 "C ·~ :::, ii: 0.15 0.1 0.05 0 l!!IINTERA Sample Date Fluoride in MW-12 ~-__J · ~ ~r\J - Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • 1 ~r j r, ( I J l • ~ 1 Detected Values Non-Detected Values 9000 8000 - 7000 6000 ::; ~ 5000 !. QI ... ~ 4000 ::, Ill 3000 2000 1000 0 ~ ;, "''o ~'1> c.,"'q 20 ::; ....... ] E 15 ::, "i: f! ::, 10 BINTERA Time concentration plots for MW-12 <Jo,'> <:JI! Sulfate in MW-12 Sample Date Uranium in MW-12 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 e Detected Values • Non-Detected Values 20 :::;-tio E. cu 15 "C ·~ :c u 10 BINTERA Time concentration plots for MW-14 Chloride in MW-14 Sample Date Fluoride in MW-14 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-14 Sulfate in MW-14 0+---~---~--~------~-------------1 ::i' ] E ::, ·2 f! :, ,i.!b°' ~o 80 60 40 BINTERA Sample Date Uranium in MW-14 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values B INTERA Time concentration plots for MW-15 Chloride in MW-15 Sample Date Fluoride in MW-15 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 Detected Values • Non-Detected Values Time concentration plots for MW-15 Sulfate in MW-15 0 +---~---------~-----------------1 ~'o°' ~o B INTERA Sample Date Uranium in MW-15 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 e Detected Values • Non-Detected Values Time concentration plots for MW-17 Chloride in MW-17 0+---~--~---~--~--~---~--~--~----1 ,.?i ... ~o ~%1NTERA Sample Date Fluoride in MW-17 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 Detected Values • Non-Detected Values Time concentration plots for MW-17 Sulfate in MW-17 0 +----.----,------,------,---,-----,----,------,-----; /'"' ~'Ii so 45 40 35 ~ 30 ] E 25 ::, ·2 I!! 20 -::::, 15 10 5 0 ~°'"' ~'Ii B INTERA Sample Date Uranium in MW-17 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 Detected Values • Non-Detected Values Time concentration plots for MW-18 Chloride in MW-18 0+---~---------~---------~------1 ::. ..... ~°'°' ~~ 0.45 0.4 0.35 0.3 ! 0.25 QI :2 ~ 0.2 :::J ii: 0.15 0.1 0.05 0 • !'l ,KOj ~~ s:,"' ~o.:,; BINTERA Sample Date Fluoride in MW-18 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 e Detected Values • Non-Detected Values Time concentration plots for MW-18 Sulfate in MW-18 :, 1500 -l-"E"-e-------l-+.1-----------1-1-----~=-----l "iio .§. J!! .l!! ~ 1000 +-------------------------------1 Sample Date Uranium in MW-18 60 ·.------------------------------~ 50 -1------------------------------l o -1----.---.----.-----.------.----.-----.-----.---1 ~°'"' ~'Ii BINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 Detected Values • Non-Detected Values Time concentration plots for MW-19 Chloride in MW-19 100 90 80 70 ::. 60 ~ .§. cu 50 "ti ·c: 0 :c 40 u 30 20 10 0 i:°'"' ~'I, Sample Date Fluoride in MW-19 1.6 ,------------------------------~ 1.4 ;-----------=--------------------1 ::. 1 ·r-----:;~~--~t-----r-....t-J~;::.~..-.;;:-f-W ... ...,.~vv-_.,,.,, ~ .§. ~ 0.8 'fL--------------11-----------------l ·c: 0 :::, li: 0.6 ·f----------------------------------1 0.4 +--------------------------------1 0.2 +--------------1-----------------1 o +-----.---~---~-----~-------------1 --S.INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 e Detected Values • Non-Detected Values ::.-...... ~ E ::, ·c f! ::> Time concentration plots for MW-19 Sulfate in MW-19 0 +---~--~---~--~--~--~---~--~------1 i:°'"' ~'Ii 20 15 10 Sample Date Uranium in MW-19 o ---~--~---~--~--~---~--~--~-------< /' ~'Ii Sample Date m lNTERA White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values 80 70 60 -so ... 'iia .§. a, 40 :5! ~ :c u 30 20 10 0 ?,!;, c°'" cJ <:)"' <:)"' B INTERA Time concentration plots for MW-20 Chloride in MW-20 Sample Date Fluoride in MW-20 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values 4500 4000 3500 3000 :.- ] 2500 QJ .... ~ :i 2000 "' 1500 1000 500 0 c°'"' ~'ti i' ~'ti 40 35 30 -25 .... } E 20 ::, ·c I! ::, 15 10 5 0 ?>"' i" c ~'ti ~'ti B INTERA Time concentration plots for MW-20 Sulfate in MW-20 Sample Date Uranium in MW-20 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values 80 70 60 -50 ... tia .s cu 40 :5! ls :c u 30 20 10 0 c°'t,. ~q; /' ~q; 20 -::;--QD .s cu 15 "O ·.::: 0 :::, u: 10 B INTERA Time concentration plots for MW-22 Chloride in MW-22 Sample Date Fluoride in MW-22 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-22 Sulfate in MW-22 0 +-----.----.-----,-----.----r-----.----.-----.------1 .:°'"' Qo; Sample Date Uranium in MW-22 0 +------,-----,------,----...-----,----..-----r----.-----t .:°'"' Qo; l!!J!INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values 35 30 25 ::; °oa 20 .§. a, "O -~ 15 :c u 10 5 0.9 0.8 0.7 0.6 ::; ...... ! 0.5 a, :5! ls 0.4 :::, ;::;: 0.3 0.2 0.1 0 !:)., ~ ~ ~,,,-¥. ..,-,$ I.BINTERA Time concentration plots for MW-23 Chloride in MW-23 Sample Date Fluoride in MW-23 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values Time concentration plots for MW-23 Sulfate in MW-23 Sample Date Uranium in MW-23 60 -----------------------------------1 } 50 ,._-------------------------------1 E ::, ·2 40 -H--------------------------------1 I? ::::, B INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 Detected Values • Non-Detected Values Time concentration plots for MW-24 Chloride in MW-24 Sample Date Fluoride in MW-24 -1 +---------------------------e-------iH.----t--M~ ~ .s a, 0.8 -1-------------------------P"---ll-... ------c::, ·;:: 0 :::, U: 0.6 ________________________ _,._ _____ -! ;J!!IINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values Time concentration plots for MW-24 Sulfate in MW-24 :::. "iio 2000 +--------------------------------1 s $ ~ :i 1500 +------------------------------- "' 250 200 :::l' 150 ] E :::, 'i: I! ::::, 100 so ' '-.. 0 BINTERA Sample Date Uranium in MW-24 A - Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 - • - Detected Values Non-Detected Values l!!!INTERA Time concentration plots for MW-24A Chloride in MW-24A Sample Date Fluoride in MW-24A Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 e Detected Values • Non-Detected Values 10 9 8 7 ::i' .:a 6 -= E 5 :::, ·2 "' .. 4 ::::, 3 2 1 0 ~ !.'~ ~ .... 'b 'f"q lil'!:2¥slNTERA Time concentration plots for MW-24A Sulfate in MW-24A Sample Date Uranium in MW-24A Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values B INTERA Time concentration plots for MW-25 Chloride in MW-25 Sample Date Fluoride in MW-25 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 e Detected Values • Non-Detected Values B INTERA Time concentration plots for MW-25 Sulfate in MW-25 Sample Date Uranium in MW-25 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values 100 90 80 70 • :::; 60 -00 .§. a, so 't, -~ :i: 40 u 30 20 10 D s;i'\. ? .,,,,<:J. ~o 1 0.9 0.8 0.7 ~ 0.6 .§. a, 0.5 't, ·c: 0 :I 0.4 u: 0.3 0.2 0.1 D s;i'\. ,r~ .,,,,q ~o IJ!!!INTERA Time concentration plots for MW-26 ~ ,,.e:J Chloride in MW-26 Sample Date Fluoride in MW-26 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 e Detected Values • Non-Detected Values Time concentration plots for MW-26 Sulfate in MW-26 -::;-1500 +------------------V:-----~---1'-----1 'ii. .5. J!l J! ~ 1000 +------------------------------1 100 -::;- l 80 E :I ·1: ~ 60 :) 40 20 ;JBINTERA Sample Date Uranium in MW-26 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 Detected Values • Non-Detected Values 1 0.9 0.8 0.7 ~ 0.6 .§. cu 0.5 "D ·~ :::, 0.4 u:: 0.3 0.2 0.1 0 !:)., ,$-~ ~'I>~ '>" ---9.INTERA Time concentration plots for MW-27 Chloride in MW-27 Sample Date Fluoride in MW-27 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values B INTERA Time concentration plots for MW-27 Sulfate in MW-27 Sample Date Uranium in MW-27 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values Time concentration plots for MW-28 Chloride in MW-28 180 160 140 120 ':a' ] 100 a, "C -~ 80 :c u 60 40 20 0 ~ ~ ~"' § ~'I>~ i: ..,-s ~'I> Sample Date Fluoride in MW-28 -0.5 ------------------<---------------..... ~ .§. a, 0.4 --------------------------------"C ·;:: 0 :I U:: 0.3 -------------------------------1 l!IINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 e Detected Values • Non-Detected Values Time concentration plots for MW-28 Sulfate in MW-28 Sample Date Uranium in MW-28 140 +----------------------1----------------1 E :::, ·2 ~ 30 .,.._ ________________________________ _, ::::, l!!INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values 45 40 35 30 :::;-....... r 25 QI "C -~ 20 :c u 15 10 5 0 s:>"' ..,.,,<1-~ ~,,,~ B INTERA Time concentration plots for MW-29 s:>°' ~~ Chloride in MW-29 Sample Date Fluoride in MW-29 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 e Detected Values • Non-Detected Values 60 so 40 } E 30 :::, "i: ~ :, 20 10 0 ---I' BINTERA Time concentration plots for MW-29 - Sulfate in MW-29 Sample Date Uranium in MW-29 ----------- Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 ---... a..._ -~ • • .,,.. Detected Values Non-Detected Values ::i' Time concentration plots for MW-30 Chloride in MW-30 Sample Date Fluoride in MW-30 <o (f ... 0 tia 0.4 -------~--------------------1-11-tt------l------l-----l .§. QI "O ·c: g 0.3 .J----..... ---------------1-A-.f--------W---ll-----'I#-~ li: B INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values Time concentration plots for MW-30 Sulfate in MW-30 800 ::. ....... OD .s 600 .2l ~ :i "' 400 Sample Date Uranium in MW-30 ::. ~ B ;~=-<.-------.+-------------..a-------a ..:!: E :I -~ 6 -J--------------------------------------1 ~ l!IINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values Time concentration plots for MW-31 Chloride in MW-31 300 +----------------------+::llF--i---il'----1 ~ 250 +------------------thil•~ .... --------<11----1 .§. QI "C -~ 200 +--------------~ .. ri-~-------------1 :l: u ::::i' Sample Date Fluoride in MW-31 ~ 0.8 f--------l-+---~lf--\::a:---A..Arlt--------1---jll-:.---A----I .§. QI :2 g 0.6 +---------<1-1-----------1--------------V-------'---=...i ii: BINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values 1400 1200 1000 ~ ~ 800 ..s QI .... J!! 600 "3 Ill 400 ~9=1NTERA Time concentration plots for MW-31 Sulfate in MW-31 Sample Date Uranium in MW-31 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 e Detected Values • Non-Detected Values ::;- tio .s Time concentration plots for MW-32 Chloride in MW-32 Sample Date Fluoride in MW-32 0.6 .--------------------------------, 0.5 -i-----------------------------1------1 0.4 ·1---------------------------..La----l {I 0.3 lk-------11-----------------------...j....-1----l ·c: 0 :::, ii: 0 -i-----,---------,---~-----r---~---~--~--~------1 IJJIINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 Detected Values • Non-Detected Values ::.-"iia E Time concentration plots for MW-32 Sulfate in MW-32 "; 1500 +------------------------------1 ... .l!! :; "' ::.- Sample Date Uranium in MW-32 "iia 4 -t---to--------------------------------1 -== E :I -~ 3 -l----l--&--..._----4_--------------------------1 ... ::::, .-$1NTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values Time concentration plots for MW-35 Chloride in MW-35 0 +------,----,-------,----,-------,----.------,----.--------1 ::; <:"'<::; ~q; Sample Date Fluoride in MW-35 "oli 0.4 ---=--=----------------------~-----""'"----------t .§. QI :2 g 0.3 +-------------1..--t----1---...... -...--------,---~...--~---w ii: B INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values 35 30 25 :::;- 120 E ::, 'i: ~ 15 ::::, 10 5 BINTERA Time concentration plots for MW-35 Sulfate in MW-35 Sample Date Uranium in MW-35 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values B INTERA Time concentration plots for MW-36 Chloride in MW-36 Sample Date Fluoride in MW-36 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-36 Sulfate in MW-36 ::. 'tin 2000 .+--------------------------------1 g ! J!! "3 1500 -1--------------------------------1 Ill 20 ::. l E 15 :::, ·c ~ ::::, 10 l!IINTERA Sample Date Uranium in MW-36 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values B INTERA Time concentration plots for MW-37 Chloride in MW-37 Sample Date Fluoride in MW-37 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values l!!INTERA Time concentration plots for MW-37 Sulfate in MW-37 Sample Date Uranium in MW-37 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 e Detected Values • Non-Detected Values Time concentration plots for MW-38 Chloride in MW-38 so 45 40 35 < 30 QI) .§. CIJ 25 :2 5 5 20 15 10 5 0 'b 'b ~~ """ iY" ~'I> 0 ~'I> Sample Date Fluoride in MW-38 1.2 -,------------------------------~ 1 -------------------------------- 0.4 -1--------------------------------,-1 0.2 ------------------------------ 0 -1-----,------,----,------,------,---..------.------,----1 l!!!INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 e Detected Values • Non-Detected Values Time concentration plots for MW-38 Sulfate in MW-38 -::i' ~ 2000 +-------------------------------1 E. s ~ :i 1500 +-------------------------------1 Ill Sample Date Uranium in MW-38 7..----------------------------------, i 6.4 ------------------+--------11------------ E :, ·2 (!! 6,2 +----.,_ ______________________ _.,_ ______ I :) 5.6 ---~---..----~------~------~--~------, ~2¥slNTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values 45 40 35 30 ::. ...... ! 25 GI 'C ·g 20 :c u 15 10 5 0 'b 'b ~ .... ti ... ~'I> 0 •1NTERA Time concentration plots for MW-39 ~l ~'I> Chloride in MW-39 Sample Date Fluoride in MW-39 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 e Detected Values • Non-Detected Values Time concentration plots for MW-39 Sulfate in MW-39 Sample Date Uranium in MW-39 _10 -1--------------------------------l ... } E 8-1--------------------------------~ :I ·2 I!! ~ 6;--------------------------------1 BINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 Detected Values • Non-Detected Values Time concentration plots for MW-40 Chloride in MW-40 Sample Date Fluoride in MW-40 0.9 -,------------------------------- ::; ~ _s 0.5 ;-----------------------------11---41o QI "O -~ 0.4 +----------------------------1---~/ ::, ;:;: 0.3 -+---------------------------_._-~ 0.2 -1-----------------------------_._---6.-l 0.1 ;------------------------------11-1-----I O+---""T""----,-----.-----.----.----~--~--~---J Sample Date Detected Values l!!INTERA White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Non-Detected Values 20 ::. ...... l E 15 :, ·c ~ ::::, 10 B INTERA Time concentration plots for MW-40 Sulfate in MW-40 Sample Date Uranium in MW-40 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • Detected Values Non-Detected Values 1400 1200 1000 ::. -800 00 .E. cu "'O -~ 600 :i: u 400 200 ll!!!INTERA Time concentration plots for TW4-24 Chloride in TW4-24 Sample Date Fluoride in TW4-24 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • e Detected Values • Non-Detected Values 800 :::;-...... l E 600 :, ·c ~ ::, 400 BINTERA Time concentration plots for TW4-24 Sulfate in TW4-24 Sample Date Uranium in TW4-24 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 2nd Quarter 2022 • • Detected Values Non-Detected Values Tab J CSV Transmittal Letter Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Goble, Kathy Weinel Wednesday, August 10, 2022 10:50 AM Phillip Goble 'Thomas Rushing'; David Frydenlund; Scott Bakken; Garrin Palmer; Logan Shumway; Jordan Christine App Transmittal of CSV Files White Mesa Mill 2022 Q2 Groundwater Monitoring Q2 2022 GW Analytical Data.csv; Q2 2022 GW Field Data.csv; Q2 2022 DTW all programs - EIM.csv Attached to this e-mail is an electronic copy of laboratory results for groundwater monitoring conducted at the White Mesa Mill during the second quarter of 2022, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel / .!lE Energy Fuels Resources (USA) Inc. Kathy Weinel Director, Regulatory Compliance t:303.389.4134 I c: I t:303.389.4125 KWeinel@energyfuels.com 225 Union Blvd., Suite 600 Lakewood, CO 80228 http://www.enerqyluels.com This e-mail is intended for the exclusive use of person(s) mentioned as the recipient(s). This message and any attached files with it are confidential and may contain privileged or proprietary information. If you are not the intended recipient(s) please delete this message and notify the sender. You may not use, distribute print or copy this message if you are not the intended recipient(s). 1