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HomeMy WebLinkAboutDRC-2021-002283 - 0901a06880e0f070Div of Waste Management and Radiation Control FEB 1 6 2021 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 ENERGYFUELS 303 974 2140 DI3C-Zo2(-002.2_6 3 www.energyfuels.com VIA Expedited Delivery February 10, 2021 Mr. Ty L. Howard Director of Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144880 Salt Lake City, UT 84116 Re: Transmittal of Annual Seeps and Springs Monitoring Report Groundwater Quality Discharge Permit UGW3700)4 White Mesa Uranium Mill Dear Mr. Howard: Enclosed are two copies of the White Mesa Uranium Mill Annual Seeps and Springs Monitoring Report for 2020 as required by the Groundwater Quality Discharge Permit UGW370004, as well as two CDs that contain a word searchable electronic copy of this report. If you should have any questions regarding this report please contact me at 303-389-4134. Yours very, truly, ENERGY FUELS RESOURCES (USA) INC. Kathy Weinel Quality Assurance Manager CC: David Frydenlund Scott Bakken Logan Shumway Terry Slade Garrin Palmer VIA Expedited Delivery February 10, 2021 Mr. Ty L. Howard Director of Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144880 Salt Lake City, UT 84116 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www.energyfuel. .c m Re: Transmittal of Annual Seeps and Springs Monitoring Report Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr. Howard: Enclosed are two copies of the White Mesa Uranium Mill Annual Seeps and Springs Monitoring Report for 2020 as required by the Groundwater Quality Discharge Permit UGW370004, as well as two CDs that contain a word searchable electronic copy of this report. If you should have any questions regarding this report please contact me at 303-389-4134. Yours very truly, -f!~'Jr~ ENERGY FUELS RESOURCES (USA) INC. Kathy Weinel Quality Assurance Manager CC: David Frydenlund Scott Bakken Logan Shumway Terry Slade Garrin Palmer White Mesa Uranium Mill 2020 Annual Seeps and Springs Sampling Report State of Utah Groundwater Discharge Permit No. UGW370004 Prepared by: 'Z'l!!I ENERGYFUELS Energy Fuels Resources (USA) Inc. 225 Union Blvd., Suite 600 Lakewood, CO 80228 February 10, 2021 Contents 1.0 INTRODUCTION .................................................................................................................................. 1 2.0 SAMPLING EVENTS ............................................................................................................................ 1 2.1 March 2020 Sampling ......................................................................................................................... 1 2.2 June 2020 Sampling ............................................................................................................................ 1 2.3 Repeat Visits to Dry Seeps and Springs .............................................................................................. 2 2.4 Sampling Procedures .......................................................................................................................... 2 2.5 Field Data ............................................................................................................................................ 3 2.6 Field QC Samples ............................................................................................................................... 3 3.0 SEEPS AND SPRINGS SURVEY AND CONTOUR MAP ................................................................. 3 4.0 QUALITY ASSURANCE AND QUALITY CONTROL. ..................................................................... 4 4.1 Laboratory Results ............................................................................................................................... 4 4.2 DATA EVALUATION ...................................................................................................................... 4 4.3 Adherence to Sampling Plan and Permit Requirements ..................................................................... 5 4.4 Analyte Completeness Review ........................................................................................................... 5 4.5 Data Validation ................................................................................................................................... 5 4.5.1 Field Data QA/QC Evaluation ..................................................................................................... 5 4.5.2 Holding Time Evaluation ............................................................................................................. 5 4.5.3 Laboratory Receipt Temperature Check ...................................................................................... 5 4.5.4 Analytical Method Check ............................................................................................................ 6 4.5.5 Reporting Limit Evaluation ......................................................................................................... 6 4.5 .6 Trip Blank Evaluation .................................................................................................................. 6 4.5.7 QA/QC Evaluation for Sample Duplicates .................................................................................. 6 4.5.8 Radiologies Counting Error ......................................................................................................... 7 4.5.9 Laboratory Matrix QC Evaluation ............................................................................................... 7 5.0 EVALUATION OF ANALYTICAL DATA .......................................................................................... 9 5.1 Evaluation of Analytical Results ......................................................................................................... 9 5.1. l Ruin Spring .................................................................................................................................. 9 5 .1.2 Cotton wood Spring ...................................................................................................................... 9 5.1.3 Westwater Seep .......................................................................................................................... 10 5.1.4 Entrance Spring .......................................................................................................................... 10 6.0 CORRECTIVE ACTION REPORT ..................................................................................................... 10 6.1 Assessment of Corrective Actions from Previous Period ................................................................. 10 7 .0 ELECTRONIC DATA FILES AND FORMAT ................................................................................... 11 8.0 SIGNATURE AND CERTIFICATION ............................................................................................... 12 II Table 1 Table 2A Table 2B Table 2C Table 2D LIST OF TABLES Summary of Seeps and Springs Sampling Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Ruin Spring Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Cottonwood Seep Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Westwater Seep Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Entrance Spring INDEX OF TABS Tab A Seeps and Springs Field Data Sheets and Photographic Documentation Tab B Field Parameter Measurement Data Tab C Survey Data and Contour Map Tab D Analytical Laboratory Data Tab E Quality Assurance and Data Validation Tables E-1 Holding Time Evaluation E-2 Laboratory Receipt Temperature Check E-3 Analytical Method Check E-4 Reporting Limit Evaluation E-5 Trip Blank Evaluation E-6 QNQC Evaluation for Sample Duplicates E-7 Radiologies Counting Error E-8 Laboratory Matrix QC Evaluation Tab F Comma Separated Values Transmittal 1l1 AWAL DR DWMRC EFRI GEL GWQS LCS Mill MS MSD Permit QA QAP QC RPD TDS voes ACRONYM LIST American West Analytical Laboratory Dry Ridge Piezometers Utah Division of Waste Management and Radiation Control Energy Fuels Resources (USA) Inc. GEL Laboratories, Inc. Groundwater Quality Standard Laboratory Control Spike White Mesa Mill Matrix Spike Matrix Spike Duplicate State of Utah Groundwater Discharge Permit No. UGW370004 Quality Assurance Groundwater Monitoring Quality Assurance Plan Quality Control Relative Percent Difference Total Dissolved Solids Volatile Organic Compounds lV ANNUAL SEEPS AND SPRINGS SAMPLING REPORT 1.0 INTRODUCTION This is the 2020 Annual Seeps and Springs Sampling Report for the Energy Fuels Resources (USA) Inc. ("EFRI") White Mesa Mill (the "Mill"), as required under Part I.F.7 of the Mill's State of Utah Groundwater Discharge Permit No. UGW370004 (the "Permit") and the Mill's Sampling and Analysis Plan for Seeps and Springs, Revision: 2, July 8, 2016 (the "Sampling Plan"). The Sampling Plan for Seeps and Springs was revised in July 2016 to incorporate changes requested by the Division of Waste Management and Radiation Control ("DWMRC"). The Sampling Plan for Seeps and Springs, Revision: 2, July 8, 2016 was approved by DWMRC by letter dated August 8, 2016. 2.0 SAMPLING EVENTS Seeps and springs which were identified near the Mill in the 1978 Environmental Report (Plate 2.6-10, Dames and Moore, January 30, 1978) are to be sampled annually in accordance with the Sampling Plan and Part I.E.6 of the Permit. The Sampling Plan specifies the following sample locations: Corral Canyon Seep, Corral Springs, Ruin Spring, Cottonwood Seep, Westwater Seep and Entrance Spring (also referred to as Entrance Seep). 2.1 March 2020 Sampling In accordance with the DWMRC-approved Sampling Plan, once per calendar quarter, Westwater Seep, Corral Canyon Seep and Corral Springs are visited to determine if there is any water for sampling. If sufficient water is present, a sample is collected and no further visits are required for the remainder of the year. Westwater Seep, was visited in mid-March 2020 and water was present. DWMRC informed EFRI that if water was noted in Westwater Seep during the first quarter, they would travel to the site in order to collect a split sample. EFRI notified DWMRC of the presence of water, however, due to COVID-19 travel restrictions, DWMRC was precluded from traveling to the Mill. EFRI collected a sample on March 25, 2020. Corral Canyon Seep and Corral Springs are discussed below. 2.2 June 2020 Sampling In accordance with the Permit and the Sampling Plan, DWMRC was notified of the annual sampling event. The DWMRC representative was present for this sampling event. On June 16, 2020, EFRI collected seeps and springs samples from Cottonwood Seep, Ruin Spring, Entrance Seep, Westwater Seep and Back Spring (duplicate of Cottonwood Seep). The DWMRC representative collected a "split" sample on June 16, 2020 from the EFRI sampling equipment, using sample containers he provided. Corral Canyon Seep and Corral Springs were dry during the annual sampling event. 1 2.3 Repeat Visits to Dry Seeps and Springs. Corral Canyon Seep and Corral Springs, were visited once per calendar quarter in 2020. The visits were conducted in February, May, July and October 2020. Corral Canyon Seep and Corral Springs, were dry during all of the visits, could not be sampled, and did not warrant development attempts with limited hand tool excavation at that time. In addition, during the June 16, 2020 sampling event, Corral Canyon Seep and Corral Springs were visited and were dry, could not be sampled, and did not warrant development attempts with limited hand tool excavation at that time. 2.4 Sampling Procedures Samples were collected and analyzed for the parameters listed in Table 2 of the Permit. Samples were collected from the locations indicated in Table 1. Sampling procedures for each seep or spring are determined by the site location and access. The DWMRC-approved sampling procedures for seeps and springs at the Mill are contained in the Sampling Plan. Samples collected under this plan were collected either by direct collection which involves collecting the sample directly into the sample container from the surface water feature or from spring out-flow, or by using a stainless steel ladle to collect water until a sufficient volume is contained in the ladle for transfer to the sample bottle. Filtered parameters are pumped through a 0.45 micron filter prior to delivery to the sample bottle. Ruin Spring In the case of Ruin Spring, sample bottles for the analytes collected during the June sampling event (except gross alpha and heavy metals) were filled directly from the spring out-flow which is a pipe. Samples for heavy metals and gross alpha were collected by means of a peristaltic pump and delivered directly to the sample containers through a 0.45 micron filter. The appropriate preservatives for the analytical technique were added to the samples. Westwater Seep For Westwater Seep, all of the sample containers were filled by means of a peristaltic pump and delivered directly to the sample containers. Samples for heavy metals and gross alpha were collected by means of a peristaltic pump and delivered directly to the sample containers through a 0.45 micron filter. The appropriate preservatives for the analytical technique were added to the samples. Cottonwood Seep and Entrance Spring Cottonwood Seep and Entrance Spring were "developed" prior to the sampling event by Field Personnel. Development was completed by removing surrounding vegetation and clearing the sampling location in the spring or seep area. The sample containers were filled by means of a peristaltic pump and delivered directly to the sample containers. In the case of the samples for heavy metals and gross alpha, the samples were delivered by a peristaltic pump directly to the 2 sample containers through a 0.45 micron filter. The samples were preserved by the addition of the appropriate preservative for the analytical technique. The tubing on the peristaltic pump that comes into contact with the sample water was disposed of between each sampling. As a result, no equipment required decontamination, and no rinsate samples were collected. 2.5 Field Data Attached under Tab A are copies of the field data sheets recorded in association with the March and June seeps and springs monitoring events. Photographic documentation of the sampling sites is also included in Tab A. Sampling dates are listed in Table 1 and field parameters collected during the sampling program are included in Tab B. 2.6 Field QC Samples The field Quality Control ("QC") samples generated during this sampling event included one duplicate per sampling event and one trip blank per shipment to each laboratory which received samples for VOCs. The duplicate samples (Back Spring) were submitted blind to the analytical laboratory. As previously stated, no rinsate blanks were collected during this sampling event as only disposable equipment was used for sample collection. 3.0 SEEPS AND SPRINGS SURVEY AND CONTOUR MAP Part I.F.7(c) of the Permit requires that a water table contour map that includes the elevations for each well at the facility and the elevations of the phreatic surfaces observed for each of the seeps and springs sampled be submitted with this annual repo1t. Tab C includes two contour maps. The contour map labeled C-1 shows the water table without the water level data associated with the dry ridge ("DR") investigation piezometers. The contour map labeled C-2 shows the water table with the water level data associated with the DR investigation piezometers. It is important to note that Cottonwood Seep is not included in any of the perched water level contouring, because there is no evidence to establish a hydraulic connection between Cottonwood Seep and the perched water system. Cottonwood Seep is located near the Brushy Basin Member/Westwater Canyon Member contact, approximately 230 feet below the base of the perched water system defined by the Burro Canyon Formation/Brushy Basin Member contact. The stratigraphic position of Cottonwood Seep indicates that its elevation is not representative of the perched potentiometric surface. Exclusion of the Cottonwood Seep from water level contouring is consistent with previous submissions. The contour map includes the corrected survey data from December 2009 as discussed below. Part I.F.7 (g) of the Permit requires that survey data for the seeps and springs be collected prior to the collection of samples. DRC previously clarified that the requirement to submit survey data applies only to the first sampling event and not on an annual basis. The December 2009 and July 2010 seeps and springs survey data shown in Tab C will be used for reporting where seeps and springs locations and elevations are relevant. 3 A full discussion of the survey data and the hydro geology of seeps and springs at the margins of White Mesa in the vicinity of the Mill and the relationship of these seeps and springs to the hydrogeology of the site, in particular to the occurrence of a relatively shallow perched groundwater zone beneath the site, is contained in Hydrogeology of the Perched Groundwater Zone and Associated Seeps and Springs Near the White Mesa Uranium Mill Site, dated November 12, 2010, prepared by Hydro Geo Chem, Inc. and submitted to the Director on November 15, 2010. Additional information is also contained in the Second Revision Hydrogeology of the Perched Groundwater Zone in the Area Southwest of the Tailings Cells White Mesa Mill Site, dated November 7, 2012, prepared by Hydro Geo Chem, Inc. and submitted to the Director on November 7, 2012. 4.0 QUALITY ASSURANCE AND QUALITY CONTROL 4.1 Laboratory Results Analytical results are provided by the Mill's two contract analytical laboratories GEL Laboratories, Inc., ("GEL") and American West Analytical Laboratory ("AWAL"). The laboratories utilized during this investigation were certified under the Environmental Lab Certification Program administered by UDEQ Bureau of Lab Improvement for the analyses they completed. The analytical data as well as the laboratory Quality Assurance ("QA")/QC summaries are included under Tab D. 4.2 DATA EVALUATION The Permit requires that the annual seeps and springs sampling program be conducted in compliance with the requirements specified in the Mill's approved White Mesa Uranium Mill Groundwater Monitoring Quality Assurance Plan ("QAP"), the approved Sampling Plan and the Permit. To meet this requirement, the data validation completed for the seeps and springs sampling program verified that the program met the requirements outlined in the QAP, the Permit and the approved Sampling Plan. The Mill QA Manager performed a QA/QC review to confirm compliance of the monitoring program with requirements of the Permit and the QAP. As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and quality control review of laboratory data methods and data. Identification of field QC samples collected and analyzed is provided in Section 4.5.1. Discussion of adherence to the Sampling Plan is provided in Section 4.3. Analytical completeness review results are provided in Section 4.4. The steps and tests applied to check laboratory data QA/QC are discussed in Sections 4.5.1 through 4.5.9 below. The analytical laboratories have provided summary reports of the analytical QA/QC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference certification and reporting protocol. The analytical laboratory QA/QC Summary Reports, including copies of the Mill's Chain of Custody and Analytical Request Record forms for each set of analytical results, follow the analytical results under Tab D. Results 4 of the review of the laboratory QA/QC information are provided under Tab E and discussed in Section 4.5 below. 4.3 Adherence to Sampling Plan and Permit Requirements On a review of adherence by Mill personnel to the Permit, the QA Manager observed that QA/QC requirements established in the Permit and the QAP were met and that the requirements were implemented as required except, as noted below. The Permit only requires the measurement of the field parameters pH, conductivity and temperature. Field parameter measurements collected during this sampling event included pH, conductivity, temperature, redox potential, and turbidity. 4.4 Analyte Completeness Review The analyses required by the Permit Table 2 were completed. 4.5 Data Validation The QAP and the Permit identify the data validation steps and data quality control checks required for the seeps and springs monitoring program. Consistent with these requirements, the QA Manager performed the following evaluations: a field data QA/QC evaluation, a receipt temperature check, a holding time check, an analytical method check, a reporting limit check, a trip blank check, a QA/QC evaluation of sample duplicates, a gross alpha counting error evaluation and a review of each laboratory's reported QA/QC information. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab E. 4.5.1 Field Data QA/QC Evaluation The QA Manager performs a review of field recorded parameters to assess their adherence with QAP and Permit requirements. The assessment involved review of the Field Data sheets. Review of the Field Data Sheets noted that the requirements for field data collection were met. 4.5.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided under Tab E. The samples were received and analyzed within the required holding time. 4.5.3 Laboratory Receipt Temperature Check Chain of Custody sheets were reviewed to confirm compliance with the sample receipt requirements specified in the QAP. Sample receipt temperature checks are provided under Tab E. The samples were received within the QAP required temperature limit. 5 4.5.4 Analytical Method Check The analytical methods reported by both laboratories were checked against the required methods specified in Table 1 of the QAP. Analytical method check results are provided in Tab E. 4.5.5 Reporting Limit Evaluation Reporting limits utilized by the laboratory were required to be equal to or lower than the GWQSs set out in Table 2 of the Permit. For Total Dissolved Solids ("TDS"), sulfate and chloride, for which Ground Water Quality Standards are not set out in Table 2 of the Permit, reporting limits specified in Part l.E.6.e).(l) were used. Those reporting limits are 10 mg/L for TDS, and 1 mg/L for Sulfate and Chloride. The analytical method reporting limits reported by both laboratories were checked against the reporting limits specified in the Permit. Reporting limit evaluations are provided in Tab E. All analytes were measured and reported to the required reporting limits except the sample results that had the reporting limit raised due to sample dilution necessary to accommodate the analyte concentrations in the samples. In all cases the reported value for the analyte was higher than the increased detection limit. 4.5.6 Trip Blank Evaluation The trip blank results were reviewed to identify any VOC sample contamination which is the result of sample handling and shipment. Trip blank evaluation is provided in Tab E. The trip blank results associated with the samples were less than reporting limit for the VOCs except for the June 16, 2020 trip blank which had a detection of 3.83 ug/L of tetrahydrofuran ("THF"). All of the samples associated with the trip blanks were nondetect for THF. The reported detections of THF in the trip blanks, but not in the associated samples indicates that the trip blanks were contaminated at the laboratory when they were made and the results are not indicative of contamination of the samples during shipping. As such, the data are usable for the intended purpose and there is no effect on the sample analytical results. 4.5.7 QA/QC Evaluation for Sample Duplicates Section 9.1.4 a) of the QAP states that the Relative Percent Difference ("RPD") will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results ( described as activities in the QAP) are less than 5 times the required detection limit. This standard is based on the United Stated Environmental Protection Agency Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for duplicate pairs for the analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits; however, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPD is greater than 20%. RPDs are also only calculated when both the sample and the duplicate report a detection for any given analyte. If only one of the pair reports a detection, the RPD cannot be calculated. The additional duplicate information is provided for information purposes. 6 All duplicate results were within 20% RPD except for TDS in the duplicate pair Cottonwood Seep/Back Spring. The TDS RPD was greater than 20%, and the sample and duplicate results reported for Ruin Spring/Back Spring were five times greater than the RLs. The approved QAP specifies a separate corrective action for duplicate RPDs outside of acceptance limits. The revised procedure for duplicate results outside of acceptance limits was implemented for the results outside of the acceptance limits. The corrective actions that were taken in accordance with the QAP procedure are as follows: the QA Manager contacted the Analytical Laboratory and requested a review of the raw data to assure that there were no transcription errors and the data were accurately repo11ed. The laboratory noted that the data were accurate and reported correctly. Reanalysis was not completed as the samples were out of holding time. The duplicate evaluation is provided in Tab E. 4.5.8 Radiologies Counting Error Section 9.14 of the QAP requires that all gross alpha analysis reported with an activity equal to or greater than the Groundwater Compliance Limits set out in the Permit (for the seeps and springs samples the Groundwater Quality Standards ["GWQS"] will be used), shall have a counting variance that is equal to or less than 20% of the reported activity concentration. An error term may be greater than 20% of the reported activity concentration when the sum of the activity concentration and error term is less than or equal to the GWQS. Section 9.4 of the QAP also requires a comparability check between the sample and field duplicate sample results utilizing the formula provided in the text. All radiological results were reported were non-detect and therefore within acceptance limits. Results of routine radiologic sample QC are provided under Tab E. 4.5.9 Laboratory Matrix QC Evaluation Section 9.2 of the QAP requires that the laboratory's QA/QC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate analytical laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, EFRI's QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided under Tab E. The lab QA/QC results from both GEL and AW AL met these requirements except as described below. A number of the seeps and springs samples had the reporting limit raised due to matrix interference and/or sample dilution. In all cases where the detection limit was increased, the concentration for the analyte was higher than the increased detection limit. 7 The check samples included at least the following: a method blank, a laboratory control spike ("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the equivalent, where applicable. It should be noted that: • Laboratory fortified blanks are equivalent to LCSs. • Laboratory reagent blanks are equivalent to method blanks. • Post digestion spikes are equivalent to MSs. • Post digestion spike duplicates are equivalent to MSDs. • For method E900.l, used to determine gross alpha, a sample duplicate was used instead of aMSD. The qualifiers, and the corresponding explanations reported in the QA/QC Summary Reports for any of the check samples for any of the analytical methods, were reviewed by the QA Manager. The QAP Section 8.1.2 requires that a MS/MSD pair be analyzed with each analytical batch. The QAP does not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the MS/MSD pair be prepared on EFRI samples only. Acceptance limits for MS/MSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the QAP requirement to analyze a MS/MSD pair with each analytical batch was met. While the QAP does not require it, the recoveries were reviewed for compliance with each laboratory's established acceptance limits. The QAP does not require this level of review and the results of this review are provided for information only. The information from the Laboratory QA/QC Summary Reports indicates that the MS/MSD recoveries and the associated RPDs for the seeps and springs samples were within acceptable laboratory limits except as noted in Tab E. The MS/MSD recoveries that were outside the laboratory established acceptance limits do not affect the quality or usability of the data, because the recoveries and RPDs above or below the acceptance limits are indicative of matrix interference most likely caused by other constituents in the samples. Matrix interferences are applicable to the individual sample results only. The requirement in the QAPs to analyze a MS/MSD pair with each analytical batch was met and as such the data are compliant with the QAP. The QAP specifies that surrogate compounds shall be employed for all organic analyses, but the QAP does not specify acceptance limits for surrogate recoveries. The analytical data associated with the routine quarterly sampling met the requirement specified in the QAP. The information from the Laboratory QA/QC Summary Reports indicates that the surrogate recoveries for the seeps and springs samples were within acceptable laboratory limits for all surrogate compounds. The QAP Section 8.1.2 requires that each analytical batch shall be accompanied by a reagent blank. Contamination detected in analysis of reagent blanks/method blanks will be used to evaluate any analytical laboratory contamination of environmental samples. The QAP specified process for evaluation of reagent/method blanks states that nonconformance will exist when blanks are within an order of magnitude of the sample results. The information from the Laboratory QA/QC Summary Reports indicates that the reagent (method) blanks for the seeps 8 and springs samples were non-detect and were therefore within the acceptance criteria specified in the QAP. Laboratory duplicates are completed by the analytical laboratories as required by the analytical method specifications. Acceptance limits for laboratory duplicates are set by the laboratories. The QAP does not require the completion of laboratory duplicates or the completion of a QA assessment of them. EFRI reviews the QC data provided by the laboratories for completeness and to assess the overall quality of the data provided. Laboratory duplicate results are provided in Tab D. 5.0 EVALUATION OF ANALYTICAL DATA As previously stated, the samples were analyzed for the groundwater compliance parameters found on Table 2 of the Permit. In addition to these laboratory parameters, the pH, temperature, conductivity, (and although not required, redox, dissolved oxygen ["DO"] and turbidity) were measured and recorded in the field. 5.1 Evaluation of Analytical Results The results of the March and June sampling events shows no evidence of Mill influence in the water produced by the seeps and springs sampled. The lack of Mill influence on seeps and springs is indicated by the fact that the parameters detected are within the ranges of concentrations for the on-site monitoring wells and for available historic data for the seeps and springs themselves. For those detected analytes, concentrations are shown in Tables 2A, 2B, 2C, and 2D. The data are compared to available historic data for each seep and spring as well as to on-site monitoring well data. Specific discussions about each seep or spring are included below. 5.1.1 Ruin Spring No VOCs or radiologies were detected. Metals and major ions were the only analytes detected. The metals detections were minimal with only molybdenum, selenium and uranium having positive detections. A comparison of the 2009 through 2019 data to the 2020 data shows that the concentrations of most detected analytes remained approximately the same with only minor changes within the limits of normal analytical deviation. The reported values for uranium, calcium, chloride, potassium, sodium, and TDS, increased from the 2019 sample results, but they are below the upper range of historic background values (where available) for the on-site monitoring wells. The differences are not significant and are most likely due to normal fluctuations due to flow rates or seasonal variations due to annual precipitation. Overall, the data reported for Ruin Spring are typical for a surface water sample with no indication of Mill influence. 5.1.2 Cottonwood Spring No VOCs or radiologies were detected. Metals and major ions were the only analytes detected. The metals detections were minimal with only uranium having a positive detection. A comparison of the 2009 through 2019 data to the 2020 data shows that the concentrations of most detected analytes remained approximately the same with only minor changes within the limits of 9 normal analytical deviation. The reported values for uranium, chloride, potassium, and sodium increased from the 2019 sample results, but they are below the upper range of historic background values (where available) for the on-site monitoring wells. The differences are not significant and are most likely due to normal fluctuations due to flow rates or seasonal variations due to annual precipitation. Overall, the data reported for Cottonwood Spring are typical for a surface water sample with no indication of Mill influence. 5.1.3 Westwater Seep No radiologies or VOCs were detected in either the March or June sample. Metals and major ions were detected in both the March and June samples. In the March sample, the metals detections were minimal with only iron, manganese, and uranium having positive detections. In the June sample, the metals detections were minimal with only manganese and uranium having positive detections. A comparison of the historic data to the 2020 data shows that the concentrations of most detected analytes remained approximately the same with only minor changes within the limits of normal analytical deviation. In the March sample, the reported values for fluoride, ammonia and TDS increased from the 2019 sample results, but they are below the upper range of historic background values (where available) for the on-site monitoring wells. In the June sample, the reported values for calcium, magnesium, potassium, sodium, sulfate, TDS and uranium increased from the 2019 sample results, but they are below the upper range of historic background values (where available) for the on-site monitoring wells. The differences are not significant and are most likely due to normal fluctuations due to flow rates or seasonal variations due to annual precipitation. Overall, the data reported for Westwater Seep are typical for a surface water sample with no indication of Mill influence. 5.1.4 Entrance Spring No VOCs or radiologies were detected. Metals and major ions were the only analytes detected. The metals detections were minimal with only uranium, manganese and selenium having positive detections. A comparison of the 2009 through 2019 data to the 2020 data shows that the concentrations of most detected analytes remained approximately the same with only minor changes within the limits of normal analytical deviation. The reported values for selenium, nitrate, sulfate and TDS increased from the 2019 sample results. The detected concentrations are below the upper range of historic background values (were available) for the on-site monitoring wells. The differences are not significant and are most likely due to normal fluctuations due to flow rates or seasonal variations due to annual precipitation. Overall, the data reported for Entrance Spring are typical for a surface water sample with no indication of Mill influence. 6.0 CORRECTIVE ACTION REPORT No corrective action reports are required for the 2020 annual sampling event. 6.1 Assessment of Corrective Actions from Previous Period No corrective action reports were required for the 2019 annual sampling event. 10 7.0 ELECTRONIC DATA FILES AND FORMAT EFRI has provided to the Director electronic copies of the laboratory results as part of the annual seeps and springs monitoring in Comma Separated Values, from the laboratory. A copy of the transmittal e-mail is included under Tab F. 11 8.0 SIGNATURE AND CERTIFICATION This document was prepared by Energy Fuels Resources (USA) Inc. Energy Fuels Resources (USA) Inc. By: Scott A. Bakken Vice President, Regulatory Affairs 12 Certification I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. ~~~ Scott A. Bakken Vice President, Regulatory Affairs Energy Fuels Resources (USA) Inc. 13 Tables Table 1: Summary of Seeps and Springs Sampling ·w.0dt OrdeF Lo~.attcm Sa11qrle Dat.ec @.wLal Sie1! J!D Dllt 0:t''la}b D9:011; Cottonwood Spring 6/16/2020 AW AL = 2006528 AW AL = 7/06/2020 GEL= 514075 GEL = 7/09/2020 Entrance Seep 6/16/2020 AW AL = 2006528 AW AL = 7/06/2020 GEL= 514075 GEL = 7/09/2020 Back Spring (Duplicate of 6/16/2020 AW AL = 2006528 AW AL = 7/06/2020 Cottonwood Spring) GEL= 514075 GEL = 7/09/2020 Ruin Spring 6/16/2020 AW AL = 2006528 AW AL = 7/06/2020 GEL= 514075 GEL = 7/09/2020 Corral Spring Not Sampled -Dry Not Sampled -Dry Not Sampled -Dry Corral Canyon Seep Not Sampled-Dry Not Sampled -Dry Not Sampled-Dry AW AL = 2003627 AWAL = 4/10/2020 Westwater Seep 3/25/20 GEL= 508151 AWAL GEL = 4/14/2020 AW AL 6/16/20 = 2006528 GEL = = 7/06/2020 514075 GEL = 7/09/2020 Table 2A Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells --Ruin Spring -Range of - Average Constituent 2009 2010 2011 2011 2012 2013 2014 2015 2016 2017 2018 2019 Historic Avg2003 May July 2020 Values for 20042 Monitoring I Wells 1 * --. ----, -,-.. ---- Major Ions (mg/1) Carbonate <l <l <l l <I <I <l <I <l <l <I <l <l --.. -Bicarbonate 233 254 241 239 237 208 204 200 193 208 202 202 186 ----.. Calcium 151 136 145 148 147 149 150 162 138 145 158 165 169 --- Chloride 28 23 25 44 28 26.3 27.1 27.4 24.4 27 .4 29.9 23.9 25.8 ND -213 27 Fluoride 0.5 0.53 0.45 0.5 0.52 0.538 <I 0.445 0.541 0.5 0.414 0.505 0.473 ND-1.3 0.6 Magnesium 32.3 29.7 30.6 31.1 31.9 32.1 35.4 31.8 31.1 30.2 33.9 45.6 36.9 ·-- Nitrogen-Ammonia 0.09 <0.05 ND <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 ---~ .. Nitrogen-Nitrate 1.4 1.7 1.7 1.6 1.6 1.56 1.54 1.31 1.64 1.55 1.35 1.56 1.39 -- Potassium 3.3 3.07 3.2 3.3 3.5 3.46 3.24 3.14 3.18 3.07 3.58 3.31 4.09 -- Sodium 104 93.4 110 111 115 118 119 126 105 113 128 128 139 -- Sulfate 528 447 486 484 464 553 553 528 490 476 547 474 469 ND-3455 521 TDS 1010 903 942 905 1000 952 984 1000 916 972 IOOO 900 1240 IOl9-5548 I053 Metals (ug/1) Arsenic <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 -- -Beryllium < 0.5 <0.5 <0.5 < 0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -- Cadmium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND-4.78 0.01 Chromium <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 -~ Cobalt <10 <10 <IO <10 <10 <10 <10 <IO <IO <10 <IO <IO <10 --- Copper <10 <IO <IO <10 <IO <IO <10 <10 <10 <IO <IO <10 <10 -- Iron <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 ND-7942 25 Lead <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- Manganese <IO <IO <IO <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ND-34,550 5 Mercury <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -- Molybdenum 17 17 16 17 16 16.1 16.0 18.3 17.8 17.2 18 20.2 18.7 -- Nickel <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 ND-61 0.05 Table 2A Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells ·---.. ---Ruin Spring . . . Range of .. Average I Constituent 2009 2010 2011 2011 2012 2013 2014 2015 2016 2017 2018 2019 2020 Historic Avg2003 May July Values for 20042 Monitoring -Wells 1 * Selenium 12.2 10 11.8 10.2 10.8 10.2 12 10 10 10.5 12.2 10.8 10.5 'ND · I D!i'S~ 12.1 . Silver <10 <10 <10 <10 <10 <10 <IO <10 <10 <10 <10 <IO <10 --- Thallium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -· .. Tin <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <!00 <100 <100 -- Uranium 9.11 8.47 9.35 8.63 8.68 9.12 9.61 9.03 8.38 8.49 9.35 9.02 9.32 Nt5 ,§9.8 JO. Vanadium <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 --" -Zinc <10 <10 <10 <10 <10 <10 <IO <10 <10 <10 <10 <10 <10 -- Radiologies (pCi/1) Gross Alpha <0.2 <0.2 <-0.3 <-0.05 <-0.09 <l.0 <l <l.0 <1.0 <LO <l.57 <1.0 <1.0 ND-3~ 0.18 voes (ug/L) Acetone <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 -- Benzene <l.0 <l.0 <l.0 <l.0 <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 --.. Carbon tetrachloride <l.0 <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 <1.0 _, - Chloroform <l.0 <1.0 <l.0 <1.0 <1.0 <l.0 <1.0 <l.0 <1.0 <LO <1.0 <1.0 <1.0 -· .. Chloromethane <1.0 <1.0 <LO <l.0 <l.0 <LO <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 <1.0 .. -- MEK <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 .. ·-- Methylene Chloride <LO <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --- Naphthalene <1.0 <l.0 <1.0 <LO <LO <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 ----Tetrahydrofuran <1.0 <1.0 <LO <LO <1.0 <1.0 <1.0 <LO <1.0 <LO <LO <1.0 <1.0 --- Toluene <1.0 <1.0 <1.0 <1.0 <l.0 <LO <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -· - Xylenes <LO <LO <l.0 <l.0 <1.0 <1.0 <1.0 <LO <1.0 <1.0 <1.0 <LO <1.0 --- 1 From Figure 3, Table 10 and Appendix B of the Revised Addendum, Back1:mund Growzdwater Quality Report: New Wells.for Denison Mines (USA) Carp's White Mesa Mill Site, San Juan County, Utah , April 30, 2008. prepared by INTERA, Inc. and Table 16 and Appendix D of the Ruvised Background Grou11d11>ater Quality Report: Existing Wells.fc,r Denison Mines ( USA) CJ1p. 's White Mesa Uranium Mill Site, San Juan County, Utah, October 2007, prepared by INTERA, Inc. 2 From Figure 9 of the Revised Addendum, Evaluation of Available Pre-Operational and Regional Background Data, Background Groundwater Quality Report: Existing Wells for Denison Mines (USA) Corp. 's White Mesa Mill Site, San Juan Couinty. Utah, November 16, 2007, prepared by INTERA, Inc. *Range of average historic values for On-Site Monitoring Wells as reported on April 30, 2008 (MW-!, MW-2, MW-3, MW-3A, MW-4, MW-5, MW-11, MW-12, MW-14, MW-15, MW-17, MW-18, MW-19, MW-20, MW-22, MW-23, MW-24, MW-25, MW-26, MW-27, MW-28, MW-29, MW-30, MW-31 and MW-32)2 - Table 2B Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Cottonwood Spring .. ! Range of Average Constituent 2009 2010 2011 2011 2012 2013 2014 2015 2016 2017 2018 2019 2020 Historic Avg 1977 May July Values for 1982 1 I Monitoring I Wells1* -. -~;;·· ~ --.. - ' --Major Ions (mg/I) - Carbonate <1 <1 <1 6 <1 <1 <l <1 <1 <l <1 <l <1 -- Bicarbonate 316 340 330 316 326 280 251 271 256 280 283 286 280 :--- Calcium 90.3 92.2 95.4 94.2 101 87.9 99.7 111 102 99.6 109 122 120 --- Chloride 124 112 113 134 149 118 128 133 138 129 153 138 146 ND-213 31 Fluoride 0.4 0.38 0.34 0.38 0.38 0.417 <l 0.318 0.466 0.344 0.282 0.249 0.233 ND-1.3 0.8 Magnesium 25 24.8 25.2 25 .2 27.7 23.6 29.0 27.5 29.5 27.1 30.2 35.3 32.9 ---- Nitrogen-<0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 0.0512 <0.05 <0.05 <0.05 <0.05 <0.05 Ammonia --- Nitrogen-Nitrate 0.1 <0.l 0.1 <0.1 <0.1 <0.1 <0.l <0.1 <0.1 0.124 0.108 <0.1 <0.1 --- Potassium 5.7 5.77 6 5.9 6.2 5.53 6.18 5.91 6.11 5.72 6.35 6.78 7.14 -- Sodium 205 214 229 227 247 217 227 251 221 213 234 268 273 -- Sulfate 383 389 394 389 256 403 417 442 443 409 428 423 417 ND-3455 ' 230 TDS 1010 900 1030 978 1040 996 968 1020 1070 1080 1080 1010 860 1019-5548 811 Metals (ug/1) Arsenic <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 --- Beryllium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -- Cadmium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND -4.78 - Chromium <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 -= --Cobalt <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 -----Copper <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 -- Iron <30 <30 53 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 ND-7942 150 Lead <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 <1.0 -- Manganese <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ND-34,550 580 Mercury <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -- Molybdenum <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 --- Nickel <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 ND-61 - Selenium <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5 <5 <5 <5 <5 <5 ND-106.5 - Table 2B Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells Cottonwood Spring --- I Range of : Average Constituent 2009 2010 2011 2011 2012 2013 2014 2015 2016 2017 2018 2019 2020 Historic Avg 1971 May July Values for 1982 1 Monitoring ' Wells1* -Silver <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ~ - Thallium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <0.5 <0.5 <0.5 <0.5 -- Tin <100 <100 <100 <]00 <100 <100 <100 <100 <100 <100 <100 <100 <100 -- Uranium 8.42 8.24 7.87 8.68 8.17 8.95 9.62 9.12 8.84 9.17 10.3 10.1 10.5 ND-59.8 - Vanadium <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 -- Zinc <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 , I --- Radiologies (pCi/1) Gross Alpha <0.2 <0.2 <0.1 <-0.1 <-0.2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND-36 7.2 voes (ug/L) Acetone <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 " Benzene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Carbon <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - tetrachloride -,. Chloroform <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 "'--- Chloromethane <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --- MEK <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 --I -.. Methylene ; Chloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- Naphthalene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ---- Tetrahydrofuran <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ----.. Toluene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --· I -- ~~ . . Xylenes <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --- 1 From Figure 3, Table 10 and Appendix B of the Revised Addendum, Background Groundwater Quality Report: New Wellsji1r Denison Mines (USA) Corp 's White Mesa Mill Site, San Juan County. Utah , April 30, 2008, prepared by INTERA, Inc. and Table 16 and Appendix D of the Revised Background Groundwater Quality Report: Existing Wells for Denison Mines (USA) Corp. 's White Mesa Uranium Mill Site, San Juan County, Utah, October 2007, prepared by INTERA, Inc. *Range of average historic values for On-Site Monitoring Wells as reported on April 30, 2008 (MW-l, MW-2, MW-3, MW-3A, MW-4, MW-5, MW-1 l, MW-12, MW-14, MW-15, MW-17, MW-18, MW-19, MW-20, MW-22, MW-23, MW-24, MW-25, MW-26, MW-27, MW-28, MW-29, MW-30, MW-31 and MW-32) - I Table 2C Detected Constituents and Comparison to Historic Values and Mill Site Monitorin_e Wells Westwater.Seep -----. ' --· -Range of Average Constituent 2009 2010 2011 May 2011 July 2012 2013 2014 2015 2016 2017 2018 2019 2020 2020 Historic • (March) (June) Values for I Monitoring I -J ---Wells1 * ·--~ Major Ions (m!!/1) Carbonate <l <1 <1 <l <I <I <I <l <l <l -- Bicarbonate 465 450 371 359 399 369 444 450 270 450 --- Calcium 191 179 247 150 176 125 204 185 118 204 -- Chloride 41 40 21 32.6 38.0 27.5 36.2 41.6 26.6 40.6 ND-213 Fluoride 0.7 0.6 0.54 0.424 0.618 0.574 0.659 0.505 0.555 0.429 ND-1.3 Magnesium 45.9 44.7 34.7 Not Sampled Not Sampled Not Sampled Not Sampled 34 47.3 31.7 56.6 43.7 30.8 54.6 - Nitrogen-Ammonia <0.05 0.5 0.06 Dry Dry Dry Dry 0.123 <0.05 <0.05 0.0832 <0.05 0.0593 <0.05 - Nitrogen-Nitrate 0.8 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 .. Potassium 1.19 6.57 3.9 1.98 2.32 2.33 2.94 3.99 1.76 5.28 -- Sodium 196 160 112 139 185 133 218 152 117 245 .. Sulfate 646 607 354 392 573 318 580 436 307 460 ND-3455 TDS 1370 1270 853 896 1060 820 1220 1110 1200 1480 1019 · 5548 Metals(u~) Arsenic <5 <5 12.3 <5.0 <5 .0 <5.0 <5.0 <5.0 <5.0 <5.0 .. Beryllium <0.5 <0.5 0.91 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 - Cadmium <0.5 <0.5 0.9 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND-4.78 Chromium <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 -.. - Cobalt <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 - Copper <10 <10 16 <10 <10 <10 <10 <10 <10 <10 - Iron 89 56 4540 • <30 40.1 181 575 1200 401 <30 ND-7942 Lead <1.0 <l.0 41.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Manganese 37 87 268 171 55.5 144 312 528 369 35.4 ND-34,550 Mercury <0.5 <0.5 <0.5 Not Sampled Not Sampled Not Sampled Not Sampled <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Dry Dry Dry Dry ---Molybdenum 29 29 <10 <10 <10 <10 <10 <10 <10 <10 - Nickel <20 <20 29 <20 <20 <20 <20 <20 <20 <20 ND-61 Selenium <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 ND· 106.5 Silver <10 <10 <10 <10 <10 <10 <10 <10 <IO <10 - Thallium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 - Tin <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 - Uranium 15.l 46.6 6.64 2.1 19.0 5.17 13.2 4.92 2.34 12.90 ND -59.8 Vanadium <15 <15 34 <15 <15 <15 <15 <15 <15 <15 -- Zinc <10 <10 28 <10 <10 <10 <10 <10 <10 <10 .- Table 2C Detected Constituents and Comparison to Historic Values and Mill Site Monitorin_g Wells -----Westwater Seep -.. -·-Range of Average Constituent 2009 2010 2011 May 2011 July 2012 2013 2014 2015 2016 2017 2018 2020 2020 Historic 2019 (March) (June) Values for ! Monitoring :.. : -· Wells1 * RadiollH!ics (pCi/1) ---- Gross Alpha < -0.l <0.3 0.5 Not Sampled Not Sampled Not Sampled Not Sampled <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND-36 Dry Dry Dry Dry VQ~(ugll,) Acetone <20 <20 <20 <20 <20 23.1 <20 <20 <20 <20 - Benzene <1.0 <LO <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Carbon tetrachloride <l.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ---. Chloroform <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- Chloromethane <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 -- MEK <20 <20 <20 Nor Sampled Not Sampled Not Sampled Not Sampled <20 <20 <20 <20 <20 <20 <20 Dry Dry Dry Dry -- Methylene Chloride <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <l.0 <1.0 <1.0 -- Naphthalene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 -- Terrahydrofuran <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <l.0 <l.0 <1.0 -- Toluene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- Xylenes <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <l.0 <1.0 <1.0 <1.0 -- From Figure 3, Table 10 and Appendix B of the Revised Addendum. Background Groundwater Quality Report: New Well.tfor Denison Mines (USA ) Corp's White Mesa Mill Site, San Juan County, Utah , April 30, 2008, prepared by INTERA, Inc. and Table 16 and Appendix D of the Revised Background Groundwater Quality Report: Existing Wells for Denison Mines (USA) Corp. 's White Mesa Uranium Mill Site, San Juan County, Utah, October 2007, prepared by INTERA, Inc. *Range of average historic values for On-Site Monitoring Wells as reported on April 30, 2008 (MW-1, MW-2, MW-3, MW-3A, MW-4, MW-5, MW-11, MW-12, MW-14, MW-15, MW-I 7, MW-18, MW-19, MW-20, MW-22, MW-23, MW-24, MW-25, MW-26, MW-27, MW-28, MW-29, MW-30, MW-31 and MW-32) Table 20 Detected Constituents and Comparison to Historic Values and Mill Site Monitoria~ Wells --. Entrance Sp~ . --- Range of Average Constituent 2009 2010 2011 May 2011 July 2012 2013 2014 2015 2016 2017 2018 2019 2020 Historic Values I for Monitoring Wells1 * ---. --· -l -~ - Major Ions (mg/I) -- Carbonate <l <l <l 7 <1 <I <1 <l <I <I <I <1 <I -- Bicarbonate 292 332 270 299 298 292 247 324 340 402 236 480 242 - Calcium 90.8 96.5 88.8 96.6 105 121 103 131 131 129 116 155 144 - Chloride 60 63 49 64 78 139 76.8 75.6 75 84.6 75.9 104 76.7 ND-213 Fluoride 0.7 0.73 0.58 0.58 0.64 0.71 <1 0.606 0.668 0.615 0.454 0.912 0.638 ND-1.3 Magnesium 26.6 28.9 26.4 28.4 32.7 43 34.9 33.3 38.6 36.4 42.4 48.0 45.1 - Nitrogen-Ammonia 0.28 <0.05 <0.05 0.32 <0.05 <0.05 <0.05 0.202 0.0962 0.247 0.102 0.168 <0.05 .. . Nitrogen-Nitrate 1.4 1 1.4 0.5 2.8 2.06 3.65 <0.1 0.403 <I 2.34 <l 2.46 -- Potassium 2.4 2.74 2.6 2.9 2 3.83 1.56 l.62 <1.0 3.88 3.64 4.66 4.31 .. Sodium 61.4 62.7 62.5 68.6 77.4 127 78.9 93.1 90.8 90.3 96 126 108 -- Sulfate 178 179 166 171 171 394 219 210 245 187 243 160 317 ND-3455 TDS 605 661 571 582 660 828 688 680 828 752 820 892 964 1019 -5548 Me,~(ug/1) Arsenic <5 <5 <5 <5 <5 <5 <5 5.02 <5 9.16 <5 8.94 <5 -- Beryllium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -- Cadmium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND-4.78 Chromium <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 -- Cobalt <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 - Conner <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 - Iron <30 <30 37 55 34 162 37.2 295 94.4 371 <30 453 <30 ND-7942 Lead <1.0 <l.0 <l.0 <l.0 <1.0 <1.0 <1.0 <l.0 <l.0 <1.0 <1.0 <l.0 <l.0 - Manganese 54 11 47 84 <10 259 16.1 367 210 913 405 587 56.3 ND-34,550 Mercury <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 - Molybdenum <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 14.30 <10 I - Nickel <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 ND-61 Selenium 12.1 9.2 13.1 5.5 13.2 11.2 15.9 <5 <5 <5 15.3 <5 15 ND-106.5 Silver <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 - Thallium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 --:: Tin <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 - Uranium 15.2 17.8 18.8 15.3 21.1 38.8 23.2 36 22.0 14.6 27.6 70.1 24.7 ND-59.8 Vanadium <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 -- Zinc <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 - Table 20 Detected Constituents and Comparison to Historic Values and Mill Site Monitorine;_ Wells -Entrance Spring --.. Range of Average Constituent 2009 2010 2011 May 2011 July 2012 2013 2014 2015 2016 2017 2018 2019 2020 Historic Values for Monitoring Wells1* ·-- Radiologjcs (pCiil) - Gross Aloha 0.9 <0.5 1.5 1.6 0.5 I 2.3 <I I 3.05 <I 2.53 <l 2.63 <1 ND-36 VOCS(ue/L) Acetone <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 - Benzene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- Carbon tetrachloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- Chloroform <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- Chloromethane <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - MEK <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 - Methylene Chloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Naphthalene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Tetrahydrofuran <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Toluene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.32 <1.0 <1.0 13.1 <1.0 5.59 <1.0 -- Xylenes <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- 1 From Figure 3, Table 10 and Appendix B of the Revised Addendum, Background Groundwater Quality Report: New Wells for Denison Mines (USA) Carp's White Mesa Mill Site, San Juan County, Utah, April 30, 2008, prepared by INTERA, Inc. and Table 16 and Appendix D of the Revised Background Groundwater Quality Report: Existing Wells for Denison Mines (USA) Corp. 's White Mesa Uranium Mill Site, San Juan County, Utah, October 2007, prepared by INTERA, Inc. *Range of average historic values for On-Site Monitoring Wells as reported on April 30, 2008 (MW-1, MW-2, MW-3, MW-3A, MW-4, MW-5, MW-11 , MW-12, MW-14, MW-15, MW-17, MW-18, MW-19, MW-20, MW-22, MW-23, MW-24, MW-25, MW-26, MW-27, MW-28, MW-29, MW-30, MW-31 and MW-32) INDEX OF TABS Tab A Seeps and Springs Field Data Sheets and Photographic Documentation Tab B Field Parameter Measurement Data Tab C Survey Data and Contour Map Tab D Analytical Laboratory Data Tab E Quality Assurance and Data Validation Tables E-1 Holding Time Evaluation E-2 Laboratory Receipt Temperature Check E-3 Analytical Method Check E-4 Reporting Limit Evaluation E-5 Trip Blank Evaluation E-6 QA/QC Evaluation for Sample Duplicates E-7 Radiologic Counting Error E-8 Laboratory Matrix QC Evaluation Tab F CSV Transmittal Tab A Seeps and Springs Field Data Sheets and Photographic Documentation ~ ...... d Data Record-Seeps and Springs S~1.a.1pling Seep or Spring Location: {.. o±±al\ tN ...... OoLL.W.ti..___S....,..p .... c-'-'i Cl ...... j.>C\------------- 09'-15 Date For Initial Sampling Visit: C:./ )b/ :)...o;2.t) Time: ---------- Sample Collected: ~ Yes o No Date For Second Sampling Visit: Time: ---------------- Sample Collected: o Yes D No Date For Third Sampling Visit: ____ _ Time: ---------- Sample Collected: o Yes D No Date For Fourth Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes D No (?wM R.C) Deen L'j~M, Dc"l.11 ~~11Jer..son , Pl-.:1 6-o.b/-(. Sampling Personnel: ....r;_ Weather Conditions at Time of Sampling: _________ _ Estimated Seep or Spring Flow Rate: ,)~ (rP M O . 2:-5 Field Parameter Measurements: -pH 7.0 -Temperature (°C) _.l,__b~· :S.....__b _________ _ -Conductivity µMHOC/cm -"-'l b._7,_~...__ _______ _ -Turbidity (NTU) (if measured)_l,_. -'--l --------· -Redox Potential Eh (mV) (if measured) _)=7 ...... 7..___ ____ _ Do 5D Analytical Parameters/Sample Collection Method: Parameter Sample Taken Filtered Sam0Un2 Method - voes ~Yes D No oYes ~No Metals lll Yes oNo ~Yes DNo Nutrients 4l Yes oNo oYes ~ No Other Non eµ Yes DNo o Yes Ill No Radiologies Gross Alpha ~ Yes oNo fi.l Yes DNo QC Samples Associated with this Location: o Rinsate Blank D Duplicate Duplicate Sample Name: Direct Peristaltic Ladle Pump 0 ~ D D ~ D D III D D [$ 0 D 1¥] D s.~tc ~+ 0'/.3j ~(llM pl~s co/lec.+e; ,,.+ D'-1 '-J.5 Other ( describe in notes section) D D D D D FL .... Data Record-Seeps and Springs SaL.Ain g Seep or Spring Location: __ 8 __ =..,,~"k~-~~P-"~':j~-------------- Date For Initial Sampling Visit: Co/ I c; I )..D ;l.C) Sample Collected: ~ Yes o No Time: 0 q !.f.-5 Date For Second Sampling Visit: ________ Time: _________ _ Samp1e Collected: D Yes D No Date For Third Sampling Visit: __ _ Time: ------------ Sample Collected: D Yes D No Date For Fourth Sampling Visit: ________ Time: __________ _ Sample Collected: D Yes o No Sampling Personnel: ~en,,.. YolFJ~, LDlc)M RL-) Dee,11 L:_f1 A" 1 Dc0" J.Jc11deoo 1\1 Pl-I ; I &ob le.. Weather Conditions at Time of Sampling: _______________ _ Estimated Seep or Spring Flow Rate: _ _.,~""'·WJ,_=-· _ __.(_,_·2 ...... ~'.l..._5-L,__G--_P_M _____ _ Field Parameter Measurements: -pH -Temperature (°C) ______________ _ -Conductivity µMHOC/cm ------------ -Turbidity (NTU) (if measured) __________ _ -Redox Potential Eh (mV) (if measured) _______ _ Analytical Parameters/Sample Collection Method: Parameter Sample Taken Filtered SampUng Method voes ~ Yes DNo oYes ·~No Metals IE Yes DNo ~Yes DNo Nutrients Ii;') Yes DNo o Yes ~ No Other Non ~ Yes DNo IJ Yes !pl No Radiologies Gross Alpha ~ Yes oNo ~Yes DNo QC Samples Associated with this Location: o Rinsate Blank ~ Duplicate Duplicate Sample Name: __ Direct Peristaltic Ladle Other Pump (describe in notes section) D Iii D D D rn D D D Iii D D D Ill D D D ~ 0 D I . I F ._ .. d Data Record~Seeps and Springs Sa~wling Seep or Spring Location: -=~CLf\::..i.}_,_c"""'a ..... o.,_,c..,.,.e __ .S _____ , ... ~ ... P ____________ _ Date For Initial Sampling Visit: (;./lC:,/:).DJ...0 Sample Collected: 1211 Yes D No Time: _ ___._.! l'---'0=--5'-------- Date For Second Sampling Visit: ____________ Time: _________ _ Sample Collected: o Yes o No Date For Third Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes o No Date For Fourth Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes o No Sampling Personnel: ~aocr-Hel/,'t4j , (Dwfll~C.J De.en L::Jrv'IM , 0<!''"-1'1 He1dec4 Ph,'l &obi.:: Weather Conditions at Time of Sampling: _______________ _ Estimated Seep or Spring Flow Rate: ~ &PM Q 05 Field Parameter Measurements: -pH 7-, -Temperature (°C) -·"-'H,.a...a.,.-5._.'f __________ _ -Conductivity µMHOC/cm _...._t :U..=....:;..,~D _________ _ -Turbidity (NTU) (if measured)~'i~· "'--------- -Redox Potential Eh (m V) (if measured) _3-'~""""'1 _____ _ , D~ 77.,,,C Analytical Parameters/Sample Collection Method: Parameter Sample Taken Filtered Samplioe. Method Direct Peristaltic Ladle Other Pwnp ( describe in notes section) voes 111 Yes oNo o Yes r;; No D ljl D D Metals Iii) Yes oNo gi Yes oNo D l'j] D D Nutrients Iii Yes oNo oYes ~No D 1¥) D D Other Non ~Yes oNo oYes ell No D l¥'l D D Radiolocics Gross Alpha 00 Yes oNo ~Yes oNo D ~ D D QC Samples Associated with this Location: o Rinsate Blank o Duplicate Duplicate Sample Name: ___________ _ , t Fa..ad Data Record-Seeps and Springs Sa1upling Seep or Spring Location: _R~!A~;~O~_s-iPt-'-i-'=5--,--------------- Date For Initial Sampling Visit: b/ If,/ ~0;20 Sample Collected: i;zi Yes o No Time: !6~ Time: Date For Second Sampling Visit:_ ·---------------- Sample Collected: o Yes o No Date For Third Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes o No Time: Date For Fourth Sampling Visit: __ _ ---------------- Sample Collected: D Yes o No (._D w M ft.<...) Sampling Personnel: -"knnc.r ~,, II: Jt>.j l Dt:e11 Lj""l IA.I'\ 1 De"-"' ~et1Jcrso '1 , Pli,1 &ob le Weather Conditions at Time of Sampling: __ Estimated Seep or Spring Flow Rate: ~ & PM O . 7 0 Field Parameter Measurements: -pH Cj -Temperature (°C) __.l_.5 ............ 4_1 ___________ _ -Conductivity µMHOC/cm 132 I -~~----------Turbidity (NTU) (if measured) ()=------------ -Redox Potential Eh (mV) (if measured) -3~17~----- Do I.fl Analytical Parameters/Sample Collection Method: Parameter Sample Taken Filtered Samp~2 Method voes SJ Yes DNo o Yes ·~No Metals !Jl Yes oNo W Yes oNo Nutrients Bl Yes oNo o Yes Iii No Other Non ~ Yes DNo oYes i¥J No Radiologies Gross Alpha ~Yes oNo ~ Yes DNo QC Samples Associated with this Location: D Rinsate Blank o Duplicate Duplicate Sample Name: --- Notes: Au-:'l)d Qf'I ~;te. o.: I o LeH ::i d-c. rJ I Direct Peristaltic Ladle Other Pump (describe in notes section) &] D D D D Iii D D Iii D D D fl) D D 0 D 1¥) D D FieL ~ata Record-Seeps and Sp·rings San. ...ng Seep or Spring Location: j) e ~t I »·l o..te c Date For Initial Sampling ')sit: 3/ [).:5 / :J..D;LO Sample Collected: dYes o No SP '' ~e£P---- Time: ~ 1 ·~ob Date For Second Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes D No Date For Third Sampling Visit: ________ Time: _________ _ Sample Collected: D Yes D No Date For Fourth Sampling Visit: ________ Time: _________ _ Sample Collected: _o Yes D No Sampling Personnel: --r;; ooe,..-Won I ck I &o..q<(\ Po-.l mer Weather Conditions at Time of Sampling: !;>....,anj w .th ~me lt;,..,J Estimated Seep or Spring Flow Rate: ---=D;.._,:....,l~O.__-__.,[,.L-r: ..... P---'--M__.__ ________ _ Field Parameter Measurements: -pH -Temperature (°C) _..ul )_,_, __..qo,,.,_ ___________ _ -Conductivity µMHOC/cm ...11.1h'----------- -Turbidity (NTU) (if measured)___.O...___ -Redox Potential Eh (mV) (if measured) --...r.:~D;;t=""------ DD bl.'2. Analytical Parameters/Sample Collection Method: Parameter Sample Taken Filtered Samplin2 Method Direct Peristaltic Ladle Other Pump ( describe in notes section) voes ~Yes DNo D Yes fjl No D 00 D D Metals ~ Yes DNo Ei Yes oNo D 00 D D Nutrients ~Yes oNo oYes !Sil No D ~ D D Other Non fll Yes oNo oYes ~No D I'll D D Radiolocics Gross Alpha ~ Yes DNo 1;1;1 Yes oNo D ~ D D QC Samples Associated with this Location: o Rinsate Blank o Duplicate Duplicate Sample Name: _______________ _ noo ,h.~d Data Record-Seeps and Springs S~.tupling Seep or Spring Location: w~~+wQ\.+er See,p / 5 p(':"'j Date For Initial Sampling Visit: 6 //(,,/,)..D2 D Time:_0~8~L..~;l.5=------- Sample Collected: IJ Yes o No Date For Second Sampling Visit: __ ,----______ Time: _________ _ Sample Collected: o Yes o No Date For Third Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes o No Date For Fourth Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes D No Sampling Personnel: "iMf\cr Wo//;J:j , Weather Conditions at Time of Sampling: Estimated Seep or Spring Flow Rate: __,(H@""""·=· '--'. :___~..>...L.--'--="""-''----..... 0.e....,..,, Q,5-==-.,__ ____ _ Field Parameter Measurements: -pH (, .'iO -Temperature (°C) __._l_,._<._,_.1_;).. ____________ _ -Conductivity µMHOC/cm _I b_'1~'i _________ _ -Turbidity (NTU) (ifmeasured)_7-'-.~'--------- -Redox Potential Eh (mV) (if measured) _,,,3'-"K=5 _____ _ DO i'. b't.~ Analytical Parameters/Sample Collection Method: Parameter Sample Taken Filtered SampUni Method voes Ii! Yes oNo D Yes -~No Metals ra Yes oNo rn Yes DNo Nutrients oo Yes oNo oYes rE No Other Non l!ll Yes oNo oYes ~No Radiologies Gross Alpha ~Yes oNo ~Yes o No QC Samples Associated with this Location: D Rinsate Blank o Duplicate Direct Peristaltic Pump D Iii D ~ D CB D [fl D [jJ Duplicate Sample Name: ___________ _ Ladle Other (describe in notes section) D D D D D D D D D D ., ~ ' .. FiJ~ Jlata Record~Seeps and Springs Sarl. ...mg Date For Initial Sampling Visit: ;-l4 -ol--0 Sample Collected: o Yes ~o Date For Second Sampling Visit:____ S -l:'.;)-'J-0 Sample Collected: D Yes aJ No Date For Third Sampling Visit: 7 / 17 /;J.fJ ?..a Sample Collected: o Yes cy1. No Date For Fourth Sampling Visit: \0 /93/0-DJ...{) j Sample Collected: o Yes o No Sampling Personnel: Time: Time: Time: Time: Weather Conditions at Time of Sampling: ______ _ 130~- I~ L\1 11~'1 03~1 Estimated Seep or Spring Flow Rate: ------------------ Field Parameter Measurements: -pH -Temperature (°C) ______________ _ -Conductivity µMHOC/cm ___________ _ -Turbidity (NTU) (if measured) _________ _ -Redox Potential Eh (m V) (if measured) ______ _ Analytical Parameters/Sample Collection Method: Parameter Sample Taken Filtered Samplin2 Method voes oYes D No o Yes DNo Metals o Yes o No o Yes oNo Nutrients oYes o No o Yes oNo Other Non oYes oNo o Yes DNo Radiologies Gross Alpha D Yes oNo o Yes oNo QC Samples Associated with this Location: D Rinsate Blank o Duplicate Direct Peristaltic Pump D 0 D 0 0 0 D D D D Duplicate Sample Name: ___________ _ Notes: Ladle Other ( describe in notes section) D D D D D D D D 0 D ------------------------------- Fil.. Data Record-Seeps and Springs Sari.r..ing Date For Initial Sampling Visit: a.-1 'i-u, Time: _ _. __________ _ Sample Collected: D Yes ~o Date For Second Sampling Visit: :;, I 13 /.2..0 .. J1:!,/:J.JJ Time: __ I ~'2>~1 ............. 9, _____ _ Sample Collected: D Yes ~ No Date For Third Sampling Visit: 7 / J7 / ;1...0;1....0 Sample Collected: D Yes ~ No Date For Fourth Sampling Visit: IQ /;).3/p..o2.0 Sample Collected: D Yes atNo Sampling Personnel: Time: 0916 Time: 683/ Weather Conditions at Time of Sampling: ____ _ Estimated Seep or Spring Flow Rate: ------------------ Field Parameter Measurements: -pH -Temperature (°C) --------------- -Conductivity µMHOC/cm ___________ _ -Turbidity (NTU) (if measured) _________ _ -Redox Potential Eh (mV) (if measured) ______ _ Analytical Parameters/Sample Collection Method: Parameter Sample Taken Filtered Samplin,t Method voes D Yes DNo oYes DNo Metals D Yes DNo oYes DNo Nutrients D Yes DNo oYes oNo Other Non D Yes DNo o Yes DNo Radiologies Gross Alpha D Yes DNo DYes oNo QC Samples Associated with this Location: D Rinsate Blank o Duplicate Direct Peristaltic Pump D D D D D D D D D D Duplicate Sample Name: ----------- Notes: Ladle Other ( describe in notes section) D D D D D D D D D D ------------------------------- TabB Field Parameter Measurement Data Field parameters Ij3~ Location SampJea pH Conductivity Turbidity, Redox Temperature DO Cottonwood Spring 6/16/2020 7.09 1679 1.1 277 16.36 50 Entrance Seep 6/16/2020 7.73 1220 4.6 334 16.59 77 Back Spring (Duplicate of Cottonwood Spring) 6/16/2020 7.09 1679 1.1 277 16.36 50 Ruin Spring 6/16/2020 7.19 1321 0 317 15.91 41 Westwater Seep 3/25/2020 7.32 1176 0.0 302 11.90 61.2 Westwater Seep 6/16/2020 6.40 1644 7.7 385 16.72 64.2 TabC Survey Data and Contour Map Seeps and Springs Survey Locations Mid-December 2009 Survey Location Latitude (N) Longitude (W) Elevation FROG POND 37°33'03.5358" 109°29'04.9552 II 5589.56 CORRAL CANYON 37°33'07.1392" 109°29'12.3907" 5623.97 ENTRANCE SPRING 37°32'01.6487" 109°29'33.7005" 5559.71 CORRAL SPRINGS 37°29'37.9192" 109°29'35.8201" 5383 .35 RUIN SPRING 37°30'06.0448" 109°31'23.4300" 5380.03 COTTONWOOD 37°3 l '21.7002" 109°32'14.7923" 5234.33 WESTWATER 37°31 '58.5020" 109°31 '25.7345" 5468.23 Verification Survey July 2010 RUIN SPRING 37°30'06.0456" 109°31 '23.4181" 5380.01 COTTONWOOD 37°3 l '21.6987" 109°32'14.7927" 5234.27 WESTWATER 37°31'58.5013" 109°31'25.7357" 5468.32 @ estimated dry area TW442 temporary perched monitoring well ¢5526 installed April, 2019 showing elevation in feet amsl MW-38 perched monitoring well -Q-5463 installed February, 2018 showing elevation in feet amsl TW4-40 temporary perched monitoring well +5526 installed February, 2018 showing elevation in feet amsl M;'5~03 perched monitoring well showing elevation in feet amsl TW4-12 . . 0 5569 temporary perched monitoring well showing elevation in feet amsl TWN-7 h d ·t ·t . <>5568 temporary perc e m rate mom onng well showing elevation in feet amsl PIEZ-1 perched piezometer showing '-' 5588 elevation in feet amsl RUIN SPRING & 5380 seep or spring showing elevation in feet amsl NOTES: MW-4, MW-26, TW4-1., TW4-2, TW4-4, TW4-11, TW4-19, TW4-21, TW4-37, TW4-39, TW4-40 and TW4-41 are chloroform pumping wells; TW4-22! TW4-24, TW4-25 and TWN-2 are nitrate pumping wells; TW4-11 water level is below the base of the Burro Canyon Formation HYDRO GEO CHEM, INC. KRIGED 3rd QUARTER, 2020 WATER LEVELS (DR PIEZOMETERS NOT INCLUDED) WHITE MESA SITE APPROVED DATE REFERENCE H :/718000/nov20/ seeps_springs/Uwl0920nodr.srf FIGURE C-1 @ estimated dry area TW4-42 temporary perched monitoring well ¢ 5526 installed April, 2019 showing elevation in feet amsl MW-38 perched monitoring well -<?"5463 installed February, 2018 showing elevation in feet amsl TW4-40 temporary perched monitoring well -+-5526 installed February, 2018 showing elevation in feet amsl M:'s5so3 perched monitoring well showing elevation in feet amsl TW4-12 0 5569 temporary perched monitoring well showing elevation in feet amsl TWN-7 h d . . . .A.5568 temporary perc e nitrate monitoring V well showing elevation in feet amsl PIEZ-1 perched piezometer showing -1 5588 elevation in feet amsl RUIN SPRING & 5380 seep or spring showing elevation in feet amsl NOTES: MW-4, MW-26, TW4-1, TW4-2, TW4-4, TW4-11, TW4-19, TW4-21, TW4-37, TW4-39, TW4-40 and TW4-41 are chloroform pumping wells; TW4-22, TW4-24, TW4-25 and TWN-2 are nitrate pumpl119 wells; TW4-11 water level is below the base of the Burro Canyon Formation HYDRO GEO CHEM,INC. KRIGED 3rd QUARTER, 2020 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE H:/718000/nov20/ seeps_springs/Uwl0920dr.srf FIGURE C-2 TabD Analytical Laboratory Data INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps & Springs 2020 Lab Sample ID: 2006528-002 Client Sample ID: Ruin Spring ANAi VTICAl l ARORATORIFS Collection Date: 6/16/2020 1035h Received Date: 6/18/2020 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Arsenic mg/L 6/19/2020 1313h 7/1/2020 1327h E200.8 0.00500 < 0.00500 Beryllium mg/L 6/19/2020 1313h 7/1/2020 1351 h E200.8 0.000500 < 0.000500 Cadmium mg/L 6/19/2020 1313h 7/1/2020 1327h E200.8 0.000500 < 0.000500 Phone:(801)263-8686 Calcium mg/L 6/19/2020 1313h 7/1/2020 1905h E200.7 10.0 169 Chromium mg/L 6/19/2020 1313h 7/1/2020 1327h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 6/19/2020 13 13h 7/1/2020 1327h E200.8 0.0100 <0.0100 Fax: (801) 263-8687 Copper mg/L 6/19/2020 1313h 7/1/2020 1327h E200.8 0.0100 < 0.0100 !-mail: awal@awal-labs.com Iron mg/L 6/19/2020 1313h 7/1/2020 1351 h E200.8 0.0300 < 0.0300 Lead mg/L 6/19/2020 13l3h 7/1/2020 1351h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 6/19/2020 13 13h 7/1/2020 1905h E200.7 10.0 36.9 Manganese mg/L 6/19/2020 1313h 7/1/2020 1327h E200.8 0.0100 < 0.0100 Mercury mg/L 6/24/2020 1313h 6/25/2020 912h E245.I 0.000500 < 0.000500 Kyle F. Gross Molybdenum mg/L 6/19/2020 13 13h 7/1/2020 1327h E200.8 0.0100 0.0187 Laboratory Director Nickel mg/L 6/19/2020 1313h 7/1/2020 1327h E200.8 0.0200 < 0.0200 Potassium mg/L 6/19/2020 1313h 7/3/2020 1206h E200.7 1.00 4.09 Jose Rocha Selenium mg/L 6/19/2020 1313h 7/1/2020 1327h E200.8 0.00500 0.0105 QA Officer Silver mg/L 6/19/2020 1313h 7/1/2020 1327h E200.8 0.0100 <0.0100 Sodium mg/L 6/19/2020 1313h 7/1/2020 1905h E200.7 10.0 139 Thallium mg/L 6/19/2020 1313h 7/1/2020 135th E200.8 0.000500 < 0.000500 Tin mg/L 6/19/2020 1313h 7/1/2020 1327h E200.8 0.100 <0.100 Uranium mg/L 6/19/2020 1313h 7/1/2020 1427h E200.8 0.000300 0.00932 Vanadium mg/L 6/19/2020 1313h 7/3/2020 1206h E200.7 0.0150 < 0.0150 Zinc mg/L 6/19/2020 1313h 7/1/2020 1327h E200.8 0.0100 < 0.0100 Report Date: 7/6/2020 Page 7 of 38 All anal) ses applicable lo lhe CWA, SOWA. and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling information is located on the allached COC Confidential Business lnforrm:ition: This report is provided for lhe exclusi, e use of the ~ddressee Pri, ile~es o~ su~eq~enl ~~e of the ~?'?1e of this _con_ipany or .tn) ~mber of ils slafT. or reproducli~ ~f lhis repo~ in ~on~eclion~ wilh Lhe ~vertise~enl, P~?motio.n ~r sale of~) ~rod~cl or p~ocess, ~r in ~onn~c~ion w~Lh th~ r~-publicalion of !his report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps & Springs 2020 Lab Sample ID: 2006528-002 Client Sample ID: Ruin Spring Collection Date: 6/16/2020 1035h Received Date: 6/18/2020 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Ammonia (as N) mg/L 6/25/2020 1035h 6/25/2020 2054h E350,l 0.0500 < 0.0500 Bicarbonate (as mg/L 6/19/2020 808h SM2320B 1.00 186 CaC03) Carbonate (as CaC03) mg/L 6/19/2020 808h SM2320B 1.00 < 1.00 Phone: (801)263-8686 Chloride mg/L 6/25/2020 1926h E300.0 4.00 25.8 Toll Free: (888) 263-8686 Fluoride mg/L 6/25/2020 2156h E300.0 0.100 0.473 Fax:(801)263-8687 Ion Balance % 7/2/2020 858h Cale. -100 10.6 !-mail: awal@awal-Iabs.com Nitrate/Nitrite (as N) mg/L 6/25/2020 1243h E353.2 0.100 1.39 Sulfate mg/L 6/25/2020 1926h E300.0 30.0 469 web: www.awal-labs.com Total Anions, Measured meq/L 7/2/2020 858h Cale. 14.2 Total Cations, meq/L 7/2/2020 858h Cale. 17.6 Measured Total Dissolved Solids mg/L 6/19/2020 1209h SM2540C 20.0 1,240 Kyle F. Gross Total Dissolved Solids Cale. 1.30 7/2/2020 858h Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 7/2/2020 858h Cale. 957 Calculated QA Officer ' -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Report Date: 7/6/2020 Page l 2 of 38 All anaJyses applicable to lhe CWA SOWA. and RCRA are performed in accordance to NELAC prolocols Pertinent sampling informolion is located on the attached COC. Confidential Business Information: This report is provided for lhe exclusi,·e use of lhe ~ddressee Pri, ile~es or sub~seq~ent ~~e or the ~:u:ne of !his .con,1pany or any ~mber of its slafT, or reproductio~ ~~ this repo~ in fon~ection~ with the ~,,ertise~nt, p~~moLio.n or sale of ?'!Y ~rod~cl or p~ocess, ~r in ~nn~c~ion w(lh th~ r~-publication of Lhis report Client: Project: Lab Sample ID: ORGANIC ANALYTICAL REPORT Energy Fuels Resources, Inc. Annual Seeps & Springs 2020 2006528-002A Contact: Tanner Holliday Client Sample ID: Ruin Spring ANAi vr,c., , •ao a•roa11 s Collection Date: 6/16/2020 1035h 3440 South 700 West ,alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Received Date: 6/18/2020 11 OOh Analytical Results Analyzed: 6/19/2020 809h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Ch loromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Extracted: Dilution Factor: Test Code: 82600-W-DENlOO VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 47.7 51.9 47.1 52.7 50.00 95.5 72-151 50.00 104 80-152 50.00 94.2 72-135 50.00 105 80-124 Report Date: 7/6/2020 Page 17 of38 All anal) ses applicable lo the CWA. SOWA. and RCRA ilf'e perfonned in accordance to NE LAC protocols Pertinent stimpling information is located on Lhe aUached COC Conridenti.:il Business lnformalion: This repon is pro\'ided for !he exclusi, e use of the ~ddressee Pri \ ile~es o.f sub~seq~nt ~~e of the !~~e of Lhis .con.1pany or an, ~mber of ils staff, or reproduclio~ ~f Lhis repo~ in ~on~1eclion~ ,,·iLll lhe ™!' ertisement, P~?motio.n or sale of~;~. ~rod~cl or p~ocess, ~r in ~onn:_c~ion w~Lh th~ r~-publicalion of this report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: July 13, 2020 Company : Address: Contact: Project: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Analytical for Annual Seeps & Springs 2020 ---Client Sample ID : Ruin Spring Sample ID: Matrix: Collect Date: Receive Date: Collector: 514075002 Ground Water 16-JUN-20 10:35 19-JUN-20 Client Project: Client ID: DNMI00106 DNMI001 Parameter Qualifier Result Uncertainty -----'---MDC RL Units PF DF Analyst Date Time Batch Method -------- lad Gas Flow Proportional Counting ]FPC, Total Alpha Radium, Liquid "As Received" }ross Radium Alpha U 0.423 +/-0.231 0.741 1.00 pCi/L JXK3 07/01/20 1247 2013767 The following Analytical Methods were performed: \1ethod Descri tion Anal st Comments EPA903.0 ;urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 3arium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 95.5 (25%-125%) ~otes: :::ounting Uncertainty is calculated at the 68% confidence level (I-sigma). ;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is he greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 13 of 18 SDG: 514075 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps & Springs 2020 Lab Sample ID: 2006528-003 Client Sample ID: Cottonwood Spring ANA l VTICAl LABORATORIES Collection Date: 6/16/2020 945h Received Date: 6/18/2020 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual falt Lake City, UT 84119 Arsenic mg/L 6/19/2020 1313h 7/1/2020 1330h E200.8 0.00500 < 0.00500 Beryllium mg/L 6/19/2020 1313h 7/1/2020 1356h E200.8 0.000500 < 0.000500 Cadmium mg/L 6/19/2020 1313h 7/1/2020 1330h E200.8 0.000500 < 0.000500 Calcium mg/L 6/19/2020 I 3 I 3h 7/1/2020 1908h E200.7 10.0 120 Phone:(801)263-8686 Chromium mg/L 6/19/2020 1313h 7/1/2020 1330h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 6/19/2020 1313h 7/1/2020 1330h E200.8 0.0100 < 0.0100 Fax: (801) 263-8687 Copper mg/L 6/19/2020 13 I 3h 7/1/2020 1330h E200.8 0.0100 < 0.0100 !-mail: awal@awal-labs.com Iron mg/L 6/19/2020 1313h 7/1/2020 1356h E200.8 0.0300 < 0.0300 Lead mg/L 6/19/2020 1313h 7/1 /2020 1356h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 6/19/2020 1313h 7/1/2020 1908h E200.7 10.0 32.9 Manganese mg/L 6/19/2020 1313h 7 /l /2020 1330h E200.8 0.0100 < 0.0100 Mercury mg/L 6/24/2020 1313h 6/25/2020 923h E245.I 0.000500 < 0.000500 Kyle F. Gross Molybdenum mg/L 6/19/2020 13 l Jh 7/1/2020 1330h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 6/19/2020 1313h 7/1/2020 1330h E200.8 0.0200 < 0.0200 Potassium mg/L 6/19/2020 I 3 I 3h 7/3/2020 I 208h E200.7 1.00 7.14 Jose Rocha Selenium mg/L 6/19/2020 1313h 7/1/2020 1330h E200.8 0.00500 < 0.00500 QA Officer Silver mg/L 6/19/2020 1313h 7/1/2020 1330h E200.8 0.0100 < 0.0100 Sodium mg/L 6/19/2020 13 13h 7/1/2020 1908h E200.7 10.0 273 Thallium mg/L 6/19/2020 1313h 7/1/2020 1356h E200.8 0.000500 < 0.000500 Tin mg/L 6/19/2020 1313h 7/1/2020 1330h E200.8 0.100 < 0.100 Uranium mg/L 6/19/2020 1313h 7/1/2020 1430h E200.8 0.000300 0.0105 Vanadium mg/L 6/19/2020 1313h 7/3/2020 1208h E200.7 0.0150 < 0.0150 Zinc mg/L 6/19/2020 1313h 7 /I /2020 1330h E200.8 0.0100 < 0.0100 Report Date: 7/6/2020 Page 8 of38 All analyses applicable lo the CWA. SOWA, and RCRA are perfonned in accordance to NELAC protocols, Pertinent sampling information is located on the auached COC Confidential Business Cnformation: This report is pro,•ided for the exclush e use or the ~ddressee Pri, ile~es o~ sub .. seq~ent ~~e or lhe ~?':"e of this .co~puny or any ~rnber of ils staIT. or reproduclio~ ~f this repo~ in ~o~eclion~ wilh the a<!vertisement, P~?molio.n or sale or ?'!Y ~rod~ct or p~ocess, ~r in ~onni;c!ion w~lh lh~ r~-publication of lhis report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps & Springs 2020 Lab Sample ID: 2006528-003 Client Sample ID: Cottonwood Spring A>I" Yf lCIIC I AOO~ATOR lf S Collection Date: 6/16/2020 945h Received Date: 6/18/2020 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84119 Ammonia (as N) mg/L 6/25/2020 1035h 6/25/2020 2056h E350.l 0.0500 < 0.0500 Bicarbonate (as mg/L 6/19/2020 808h SM2320B 1.00 280 CaC03) Carbonate (as CaC03) mg/L 6/19/2020 808h SM2320B 1.00 < 1.00 Phone:(801)263-8686 Chloride mg/L 6/25/2020 2050h E300.0 5.00 146 Toll Free: (888) 263-8686 Fluoride mg/L 6/25/2020 22 l Jh E300.0 0.100 0.233 Fax: (801) 263-8687 [on Balance % 7/2/2020 858h Cale. -100 5.98 !-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 6/25/2020 1245h E353.2 0.100 < 0.100 Sulfate mg/L 6/25/2020 2050h E300.0 37.5 417 web: www.awal-labs.com Total Anions, Measured meq/L 7/2/2020 858h Cale. 18.4 Total Cations, meq/L 7/2/2020 858h Cale. 20.8 Measured Total Dissolved Solids mg/L 6/19/2020 1209h SM2540C 20.0 860 Kyle F. Gross Total Dissolved Solids 7/2/2020 858h Cale. 0.738 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 7/2/2020 858h Cale. 1,160 Calculated QA Officer Report Date: 7/6/2020 Page 13 of 38 All anal~ ses applicnble lo lhe CWA. SDWA, and RCRA are performed m accordance lo NELAC protocols Pertinent sompling informolion is loculed on the auached COC, Confidential Business Information: This report is prO\ ided for the exclusi, e use of the ~ddressee Pri\ ile~es oF sub ... seq~1enl ~~e of lhe ~~e of this .con:ipany or an~ ~mber of its slaff, or reproductio~ ~r this repo~ in ~on~eclion~ \\ ith the a~, ertisemenl. P~?motio.n or sale of ~!Y ~rod~ct or p~ocess, ~r in ':°"nt;c~ion ,v~lh lh~ r!-publicalion or this report ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Annual Seeps & Springs 2020 2006528-003A Client Sample ID: Cottonwood Spring ANAi vr,c•, , •0oa•roa1Fs Collection Date: 6/16/2020 945h 3440 South 700 West ,alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Received Date: 6/18/2020 1100h Analytical Results Analyzed: 6/19/2020 829h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Extracted: Dilution Factor: Contact: Tanner Holliday Test Code: 8260D-W-DENIOO VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Jose Rocha QA Officer Surr: l ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromotluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 47.8 53.2 46.2 53.2 50.00 95.5 72-151 50.00 106 80-152 50.00 92.3 72-135 50.00 106 80-124 Report Date: 7/6/2020 Page 18 of38 All analyses applicable lo the CWA. SDWA. and RCRA are perfom1ed in accordance to NELAC protocols. Pertinent sampling information is localed on Lhe attached COC Confidenliol Business Information: This report is pro\·ided for lhe e:xclusi\ e use of the ~ddressee. Pri, ile~es or sub .. seq~enl ~e or the ~?'.11e of this .co";pany or an~ ~mber or ils staII or reproducti~ ~r this repo~ in ~o~ecLion~ with lhe n~~·ertisemenl, P~?molio.n or saJe or ~y ~rod~cl or p~ocess, ~r in ~onn~!ion \\'!Lh 1h~ r:·publication or lhis report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: July 13, 2020 Company: Address: Contact: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Project: Analytical forAnnual Seeps & Springs 2020 Client Sample ID: Cottonwood Spring Sample ID: 514075003 Matrix: Ground Water Collect Date: 16-JUN-20 09:45 Receive Date: 19-JUN-20 Collector: Client Parameter Qualifier Result ~ncertainty MDC RL {ad Gas Flow Proportional Counting ]FPC, Total Alpha Radium, Liquid "As Received" }ross Radium Alpha U 0.256 +/-0.209 0.721 1.00 The following Analytical Methods were performed: Project: Client ID: DNMI00106 DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXK3 07/01/20 1247 2013767 ~---------------vlethod Descri tion EPA 903.0 ;urrogate/Tracer Recovery Test ~------------3 ar i um Carrier GFPC, Total Alpha Radium, Liquid "As Received" ~otes: :ounting Uncertainty is calculated at the 68% confidence level (I-sigma). Anal st Comments Result Nominal Recovery% Acceptable Limits 97.4 (25%-125%) ;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is he greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: OF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 14 of 18 SDG: 514075 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps & Springs 2020 Lab Sample ID: 2003627-001 Client Sample ID: Westwater Spring Collection Date: 3/25/2020 1300h Received Date: 3/27/2020 I IOOh Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ialt Lake City, UT 841 19 Arsenic mg/L 4/5/2020 1039h 4/7/2020 1612h E200.8 0.00500 < 0.00500 Beryllium mg/L 4/5/2020 1039h 4/7/2020 1658h E200.8 0.000500 < 0.000500 Cadmium mg/L 4/5/2020 1039h 4/7/2020 1612h E200.8 0.000500 < 0.000500 Calcium mg/L 4/5/2020 I 039h 4/6/2020 1523h E200.7 10.0 118 Phone: (801)263-8686 Chromium mg/L 4/5/2020 I 039h 4/7/2020 1612h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 4/5/2020 I 039h 4/7/2020 1612h E200.8 0.0100 < 0.0100 Fax:(801)263-8687 Copper mg/L 4/5/2020 I 039h 4/7/2020 1612h E200.8 0.0100 < 0.0100 :-mail: awal@ awal-labs.com Iron mg/L 4/5/2020 I 039h 4/7/2020 1658h E200.8 0.0300 0.401 Lead mg/L 4/5/2020 I039h 4/7/2020 1658h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 4/5/2020 I 039h 4/6/2020 1549h E200.7 1.00 30.8 Manganese mg/L 4/5/2020 I 039h 4/7/2020 1612h E200.8 0.0100 0.369 Mercury mg/L 3/27/2020 1335h 3/30/2020 I 003h E245.I 0.000500 < 0.000500 Kyle F. Gross Molybdenum mg/L 4/5/2020 I 039h 4/7/2020 1612h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 4/5/2020 I 039h 4/7/2020 1612h E200.8 0.0200 < 0.0200 Potassium mg/L 4/5/2020 I 039h 4/6/2020 1549h E200.7 1.00 1.76 Jose Rocha Selenium mg/L 4/5/2020 I 039h 4/7/2020 1612h E200.8 0.00500 < 0.00500 QA Officer Silver mg/L 4/5/2020 I 039h 4/7/2020 1612h E200.8 0.0100 < 0.0100 Sodium mg/L 4/5/2020 I 039h 4/6/2020 1523h E200.7 10.0 117 Thallium mg/L 4/5/2020 I 039h 4/7/2020 1658h E200.8 0.000500 < 0.000500 Tin mg/L 4/5/2020 I 039h 4/7/2020 1612h E200.8 0.100 < 0.100 Uranium mg/L 4/5/2020 I 039h 4/7/2020 1712h E200.8 0.000300 0.00234 Vanadium mg/L 4/5/2020 I 039h 4/7/2020 1612h E200.8 0.0150 < 0.0150 Zinc mg/L 4/5/2020 I 039h 4/7/2020 1612h E200.8 0.0100 < 0.0100 Report Date: 4/10/2020 Page 5 of 26 All ano.l) ses applicable to 1he CW A. SOW A. and RCRA are perfom1ed in accordance to NELAC protocols, Per1inen1 samplin1: information is located on Lhe attached COC Confidential Business Information: This report is pro\'ided for the exclush e use of the ~ddrcssee Pri,•ile~es or su~seq~enl ~~e of lhe ~~e of this .co1~pany or Mr 1~mber of ils slnIT, or reproductio~ ~r this repo~ in .con?eclion .. with lhe ~vertisemenl, P~?motio.n ~r sale or ?1!Y ~rod1~ct or p~ocess, ~r in ~nn:c!ion w!th th~ r:-publicalion or this report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps & Springs 2020 Lab Sample ID: 2003627-001 American West Client Sample ID: Westwater Spring ANALYTICAL LABORATORIES Collection Date: 3/25/2020 1300h Received Date: 3/27/2020 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Ammonia ( as N) mg/L 4/1/2020 846h 4/2/2020 143 lh E350.1 0.0500 0.0593 '@ Bicarbonate (as mg/L 3/31/2020 729h SM2320B 1.00 270 CaC03) Carbonate (as CaC03) mg/L 3/31/2020 729h SM2320B 1.00 < 1.00 Phone: (801) 263-8686 Chloride mg/L 4/1/2020 732h E300.0 2.00 26.6 Toll Free: (888) 263-8686 Fluoride mg/L 4/1/2020 914h E300.0 0.100 0.555 Fax: (801) 263-8687 Ion Balance % 4/6/2020 1631h Cale. -100 4.06 :-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 4/2/2020 1028h E353.2 0.100 < 0.100 Sulfate mg/L 4/1/2020 732h E300.0 15.0 307 web: www.awal-labs.com Total Anions, Measured meq/L 4/6/2020 1631h Cale. 12.6 Total Cations, meq/L 4/6/2020 1631h Cale. 13.6 Measured Total Dissolved Solids mg/L 3/30/2020 1140h SM2540C 20.0 1,200 @ Kyle F. Gross Total Dissolved Solids 4/6/2020 1631h Cale. 1.57 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 4/6/2020 163 \h Cale. 764 Calculated QA Officer @ -High RPD due to suspected sample non-homogeneity or malrix interference. 1 -Matrix spike recovery indicates matrix interference. The method is in con/rol as indicated by the LCS. Report Date: 4/10/2020 Page 6 of 26 All analyses applicable to lhe CW A. SDW A. and RCRA are perfonned in accordance to NELAC protocols, Pertinent sampling information is localed on the altached COC. Confidential Business Information: This report is pr°'•ided for the exclLLSive use or lhe ~ddressee Pri, ile~es or sub ... seq~ent ~~e of the ~~e of this .con_1pany or nny 1~~be1 of its staff, or reproductio~ ~f this repo~ in .co~1eclion ... ,1,,ilh lhe u~\•enisemenl, P~?motio.n ':r sale of ~!Y ~rod~cl or p1;ocess, ~r in ~nn:_c~ion w!lh th~ r~-publication of 1his report 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Annual Seeps & Springs 2020 2003627-00lA Client Sample ID: Westwater Spring Collection Date: 3/25/2020 1300h Received Date: 3/27/2020 11 OOh Analytical Results Analyzed: 3/27/2020 1339h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surrogate Units: µg/L Surr: l,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Extracted: Dilution Factor: CAS 17060-07-0 460-00-4 1868-53-7 2037-26-5 $ -This compound exceeded (low) the control limit for the CCV. Contact: Tanner Holliday Test Code: 8260D-W-DEN100 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 $ 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Result Amount Spiked %REC Limits Qual 51.5 50.00 103 72-151 50.5 50.00 101 80-152 48.3 50.00 96.5 72-135 48.9 50.00 97.8 80-124 Report Date: 4/10/2020 Page 7 of26 All analyses applicable to the CWA, SDWA. and RCRA are performed in accordance to NELAC protocols, Per1inent sampling information is located on the auached COC. Confidential Business Information: This repor1 is provided for the exclusive use of1he ~ddressee Pridle~es of sub .. seq~ent ~~e of lhe ~~e of I his .co1~pa11y or any ~mber of its staff, or reproductio.~ ?,f this repo~ in .co~eclion,, '"'ilh lhe ~' er1isemenl P~?moti~n ~r sale of ~r ~rod~cl or p~ocess, ~r in ~nni;c~ion w!lh 1h~ r1;-p~blicnlion or lhis report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company : Address: Contact: Project: Client Sample ID: Sample ID: _ Matrix: Collect Date: Receive Date: Collector: Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Analytical forAnnual Seeps and Spring 2020 Westwater Spring 508151001 Ground Water 25-MAR-20 13:00 31-MAR-20 Client Project: Client ID: Report Date: April 14, 2020 DNMI00106 DNMIOOI Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method -------------------------------- lad Gas Flow Proportional Counting ]FPC, Total Alpha Radium, Liquid "As Received" }ross Radium Alpha U 0.559 +/-0.300 0.926 LOO pCi/L JXK3 04/13/20 1310 1987404 The following Analytical Methods were performed: \1ethod Description Anal st Comments EPA 903.0 ,urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits ---='-----------=---------------------------3a r i um Carrier GFPC, Total Alpha Radium, Liquid "As Received" 101 (25%-125%) "Jotes: :ounting Uncertainty is calculated at the 68% confidence level (I-sigma). ,RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is he greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 11 of 13 SDG: 508151 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps & Springs 2020 Lab Sample ID: 2006528-00 I Client Sample ID: Westwater Seep 0,41 H C•l I ~001U.TO!tl [8 Collection Date: 6/16/2020 845h Received Date: 6/18/2020 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Arsenic mg/L 6/19/2020 131 Jh 7/1/2020 1314h E200.8 0.00500 < 0.00500 Beryllium mg/L 6/19/2020 1313h 7/1/2020 1348h E200.8 0.000500 < 0.000500 Cadmium mg/L 6/19/2020 1313h 7/1/2020 1314h E200.8 0.000500 < 0.000500 Calcium mg/L 6/19/2020 1313h 7/1/2020 1851h E200.7 10.0 204 Phone: (801) 263-8686 Chromium mg/L 6/19/2020 1313h 7/1/2020 1314h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 6/19/2020 1313h 7/1/2020 1314h E200.8 0.0100 < 0.0100 Fax: (80 I) 263-8687 Copper mg/L 6/19/2020 1313h 7/1/2020 1314h E200.8 0.0100 < 0.0100 !-mail: awal@awal-labs.com Iron mg/L 6/19/2020 1313h 7/1/2020 1348h E200.8 0.0300 < 0.0300 Lead mg/L 6/19/2020 131 Jh 7/1/2020 1348h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 6/19/2020 131 Jh 7/1/2020 1851 h E200.7 10.0 54.6 Manganese mg/L 6/19/2020 1313h 6/22/2020 1135h E200.8 0.0100 0.0354 Mercury mg/L 6/2412020 1313h 6125/2020 910h E245.l 0.000500 < 0.000500 Kyle F. Gross Molybdenum mg/L 6/1912020 1313h 711/2020 1314h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 6/1912020 1313h 7/1/2020 1314h E200.8 0.0200 < 0.0200 Potassium mg/L 6/19/2020 1313h 7/3/2020 1158h E200.7 1.00 5.28 Jose Rocha Selenium mg/L 6119/2020 1313h 7/112020 1314h £200.8 0.00500 < 0.00500 QA Officer Silver mg/L 6/19/2020 1313h 7/112020 1314h E200.8 0.0100 < 0.0100 Sodium mg/L 6/19/2020 1313h 7/1/2020 1851h E200.7 10.0 245 Thallium mg/L 6/19/2020 1313h 7/112020 1348h E200.8 0.000500 < 0.000500 Tin mg/L 6/1912020 131 Jh 71112020 1314h E200.8 0.100 <0.100 Uranium mg/L 6/1912020 1313h 7/112020 1424h E200.8 0.000300 0.0129 Vanadium mg/L 6/19/2020 1313h 7/3/2020 1158h E200.7 0.0150 < 0.0150 Zinc mg/L 6/19/2020 1313h 7/1/2020 1314h E200.8 0.0100 < 0.0100 1 -Analyte concentralion is too high for accurate matrix spike recovery and/or RPD. Report Date: 7/6/2020 Page 6 of 38 All analyses applicable to the CWA, SDWA. and RCRA are performed in accordance Lo NELAC protocols. Pertinent sampling informalion is localed on the allached COC Confidential Business Information: This repon is pro\'ided for the exclusi,e use or the ~ddressee Pri, ile~es o~ sub .. seq~enl ~1~e of the ~~e of this .con:1pan~ or an~ ~mber of its staff, or reproductio~ ~f lhis repo~ in ~on~ection .. ,\ilh the n~rertise~enl, P~?motio.n ~r sale of ~y ~rod~cl or p~ocess, ~r in 7onn:c~ion w~Lh th~ r:·publicution or lhis report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps & Springs 2020 Lab Sample ID: 2006528-00 I Client Sample ID: Westwater Seep ",J,111,1 VTICAI I AbO A,'1,tOlHf S Collection Date: 6/16/2020 845h Received Date: 6/18/2020 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual )alt Lake City, UT 84119 Ammonia (as N) mg/L 6/25/2020 I 035h 6/25/2020 2048h E350.l 0.0500 < 0.0500 Bicarbonate (as mg/L 6/19/2020 808h SM23208 1.00 450 CaC03) Carbonate (as CaC03) mg/L 6/19/2020 808h SM23208 1.00 < 1.00 Phone:(801)263-8686 Chloride mg/L 6/25/2020 1909h E300.0 4.00 40.6 Toll Free: (888) 263-8686 Fluoride mg/L 6/25/2020 2 l 40h E300.0 0.100 0.429 Fax: (801) 263-8687 Ion Balance % 7/2/2020 858h Cale. -100 12.7 !-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 6/25/2020 l 242h E353.2 0.100 < 0.100 Sulfate mg/L 6/25/2020 1909h E300.0 30.0 460 web: www.awal-labs.com Total Anions, Measured meq/L 7/2/2020 858h Cale. 19.7 Total Cations, meq/L 7/2/2020 858h Cale. 25.5 Measured Total Dissolved Solids mg/L 6/19/2020 1209h SM2540C 20.0 1,480 Kyle F. Gross Total Dissolved Solids 7/2/2020 858h Cale. 1.16 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 7/2/2020 858h Cale. 1,280 Calculated QA Officer Report Date: 7/6/2020 Page 11 of38 All anal) ses applicable Lo the CWA. SDWA. and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on Lhe auached COC. Confidential Business Information: This report is provided for the exclusi,e use of the !ddressee Pri, ile~es o_f sub,;eq~ent ~~e of !he ~~e or I his .co"!pany or an) ~mber or ils staff. or reproduclio~ ~f this repo~ in ~on~ectio~ \\ilh the a~vertisemenl, P~?motio 1 n or sale or~) rrod~cl or P~?cess, ?r in ~onn:c~ion "!lh th; r~-publicalion of this report 3440 South 700 West ;alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Annual Seeps & Springs 2020 2006528-00IA Client Sample ID: Westwater Seep Collection Date: 6/16/2020 845h Received Date: 6/18/2020 11 OOh Analytical Results Analyzed: 6/19/2020 749h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Extracted: Dilution Factor: Contact: Tanner Holliday Test Code: 8260D-W-DEN100 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 7 l-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Surr: l,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 46.7 51.4 46.4 52.0 50.00 93.4 72-151 50.00 103 80-152 50.00 92.8 72-135 50.00 104 80-124 Report Date: 7/6/2020 Page 16 of38 All analyses applicable lo the CWA, SOWA. and RCRA are performed in accordance Lo NELAC protocols. Per1inenl sampling information is localed on lhe altached COC Confidential Business rnformalion: This report is prO\'ided for the exclusi\ e use or the !ddressee. Pri, ile~es o_fsub~seq~enl ~e or the ~~e of this .con:ipany or anr ~mber of its staff, or reproduclio~ ~f lhis repo~ in ~o~ection,, wilh lhe ~vertisemenl, P~?molio.n or sale of ~y ~rod~cl or P~?cess. ~r in ~onn~c!ion w~th th~ r:-publication of this report Company: Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Analytical forAnnual Seeps & Springs 2020 Westwater Seep 514075001 Ground Water 16-JUN-20 08:45 19-JUN-20 Client ----Project: Client ID: Report Date: DNMI00106 DNMIOOI July 13, 2020 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method -----------{ad Gas Flow Proportional Counting 3FPC, Total Alpha Radium, Liquid "As Received" }rossRadiumAlpha U 0.119 +/-0.191 0.721 1.00 pCi/L JXK3 07/01/20 1247 2013767 The following Analytical Methods were performed: \1ethod Descri tion ____________________ An~al.Y.st Comm~nts EPA 903.0 1urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 3arium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 87.9 (25%-125%) ~otes: :ounting Uncertainty is calculated at the 68% confidence level (I-sigma). 1RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is he greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 12 of 18 SDG: 514075 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps & Springs 2020 Lab Sample ID: 2006528-004 Client Sample ID: Entrance Seep u a L~11c At 1 ~ooq .. ron 11 s Collection Date: 6/16/2020 1105h Received Date: 6/18/2020 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84119 Arsenic mg/L 6/19/2020 1313h 7/1/2020 1333h E200.8 0.00500 < 0.00500 Beryllium mg/L 6/19/2020 I 3 I 3h 7/1/2020 1359h E200.8 0.000500 < 0.000500 Cadmium mg/L 6/19/2020 1313h 7/1/2020 1333h E200.8 0.000500 < 0.000500 Phone: (801) 263-8686 Calcium mg/L 6/19/2020 1313h 7/1/2020 1910h E200.7 10.0 144 Chromium mg/L 6/19/2020 1313h 7/1/2020 1333h E200.8 0.0250 < 0.0250 foll Free: (888) 263-8686 Cobalt mg/L 6/19/2020 1313h 7/1/2020 1333h E200.8 0.0100 < 0.0100 Fax: (801) 263-8687 Copper mg/L 6/19/2020 13 I 3h 7/1/2020 I 333h E200.8 0.0100 <0.0100 ~-mail: awal@awal-labs.com Iron mg/L 6/19/2020 1313h 7/1/2020 1359h E200.8 0.0300 < 0.0300 Lead mg/L 6/19/2020 1313h 7/1/2020 1359h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 6/19/2020 131 Jh 7/1/2020 1910h E200.7 10.0 45.1 Manganese mg/L 6/19/2020 1313h 7/1/2020 1333h E200.8 0.0100 0.0563 Mercury mg/L 6/24/2020 1313h 6/25/2020 925h E245.I 0.000500 < 0.000500 Kyle F. Gross Molybdenum mg/L 6/19/2020 13 I 3h 7/1/2020 1333h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 6/19/2020 131 Jh 7/1/2020 1333h E200.8 0.0200 < 0.0200 Potassium mg/L 6/19/2020 I 3 I 3h 7/3/2020 121 lh E200.7 l.00 4.31 Jose Rocha Selenium mg/L 6/19/2020 13 I 3h 7/1/2020 1333h E200.8 0.00500 0.0150 QA Officer Silver mg/L 6/19/2020 1313h 7/1/2020 1333h E200.8 0.0100 <0.0100 Sodium mg/L 6/19/2020 1313h 7/1/2020 1910h E200.7 10.0 108 Thallium mg/L 6/19/2020 I 313h 7/1/2020 1359h E200.8 0.000500 < 0.000500 Tin mg/L 6/19/2020 1313h 7/1/2020 1333h E200.8 0.100 < 0.100 Uranium mg/L 6/19/2020 1313h 7/1/2020 1433h E200.8 0.000300 0.0247 Vanadium mg/L 6/19/2020 I 3 I 3h 7/3/2020 121 lh E200.7 0.0150 < 0.0150 Zinc mg/L 6/19/2020 1313h 7/1/2020 1333h E200.8 0.0100 < 0.0100 Report Date: 7/6/2020 Page 9 of38 All analyses applicable to Lhe CWA. SDWA. and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on Lhe attached COC Confidenlinl Business Information: This repon is pro\'ided for the exclusi\e use of the ~ddressee Pri, ile~es o:sub~seq~tenl ~e of the ~~e of lhis _co~pan~ or an~ ~mber of iLs slaIT. or reproduclio~ ~f lhis repo~ in .con~ection~ with lhe a~vertisemenl. P~?moli°:" or sale or~~ ~rod~cl or p~ocess. ~r in ~onn:c!ion \\!th lh~ r:-publication of this report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps & Springs 2020 Lab Sample ID: 2006528-004 Client Sample ID: Entrance Seep Collection Date: 6/16/2020 1105h Received Date: 6/18/2020 l lOOh Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Ammonia (as N) mg/L 6/25/2020 I 035h 6/25/2020 2057h E350.l 0.0500 < 0.0500 Bicarbonate (as mg/L 6/19/2020 808h SM2320B 1.00 242 CaC03) Carbonate (as CaC03) mg/L 6/19/2020 808h SM2320B 1.00 < 1.00 Phone: (801) 263-8686 Chloride mg/L 6/25/2020 2 !06h E300.0 2.00 76.7 Toll Free: (888) 263-8686 Fluoride mg/L 6/25/2020 2247h E300.0 0.100 0.638 Fax: (80 I) 263-8687 Ion Balance % 7/2/2020 858h Cale. -100 7.00 !-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 6/25/2020 1359h E353.2 0.100 2.46 Sulfate mg/L 6/25/2020 2106h E300.0 15.0 317 web: www.awa1-labs.com Total Anions, Measured meq/L 7/2/2020 858h Cale. 13.7 Total Cations, meq/L 7/2/2020 858h Cale. 15.7 Measured Total Dissolved Solids mg/L 6/19/2020 1209h SM2540C 20.0 964 Kyle F. Gross Total Dissolved Solids 7/2/2020 858h Cale. 1.14 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 7/2/2020 858h Cale. 843 Calculated QA Officer Report Date: 7/6/2020 Page 14 of 38 All anal~ses applicable to lhe CWA. SDWA. and RCRA are perfom,ed in accordonce lo NELAC prolocols Pertinent sampling informal ion is located on 1he attached COC Conridentinl Business Information: This report is prO\'ided for the exclusive use or the ~ddressee. Pri, i\e~es o:sub,.seq~enl ~e or1he ~~,e of this .co"'}pany or an~ ~'?1ber of ils staff. or reproducti~ ~~this repo~ in ~on~eclion~ with the n~,er1isemenl, P~?moti~n or sale of~~·. ~rod~cl or p~ocess, ~r in 7onn:_c~ion 1v!Lh th~ r:_-publicalion or this report 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801) 263-8686 foll Free: (888) 263-8686 Fax: (80 I) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Annual Seeps & Springs 2020 2006528-004A Client Sample ID: Entrance Seep Collection Date: 6/16/2020 1105h Received Date: 6/18/2020 11 OOh Analytical Results Analyzed: 6/19/2020 850h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Extracted: Dilution Factor: Contact: Tanner Holliday Test Code: 8260D-W-DENIOO VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 47.4 50.00 52.7 50.00 46.2 50.00 52.9 50.00 94.8 72-151 105 80-152 92.5 72-135 106 80-124 Report Date: 7/6/2020 Page 19 of38 All analyses applicable 10 lhe CWA. SDWA. and RCRA are performed in accordance to NELAC prolocols Per1inenL sampling inrormation is located on the auached COC Confidential Business Informalion: This report is provided for !he exclusi,e use of lhe ~ddressee Pri,·ile~es o~ sub ... seq~nl ~e of the ~~e of this .con_ipnny or M) ~mber or its staff, or reproductio~ ~! this repo~ in :on~eclion ... \\ilh the ~\'ertisement, P~?moli°:'1 or saJe of :1'2.Y ~rod~ct or pi;ocess, ~r in ~onn:_cfion \\'!lh th~ r~-publication of this report Company: Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Analytical for Annual Seeps & Springs 2020 Entrance Seep 514075004 Ground Water l 6-JUN-20 11 :05 19-JUN-20 Client ----Project: Client ID: Report Date: DNMI00106 DNMIOOI July 13, 2020 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method -"--------------- lad Gas Flow Proportional Counting }FPC, Total Alpha Radium, Liquid "As Received" }ross Radium Alpha U 0.453 +/-0.229 0.722 1.00 pCi/L JXK3 07/01/20 1247 2013767 The following Analytical Methods were performed: \1ethod ----------------~A~n~~,Jyst Comments ;urrogate/Tracer Recovery Test ___________ R_e_s_u_lt __ N_o_m_in_a_l __ R_e_c_o_v_ery,% Acceptable Limits 3arium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 95.5 (25%-125%) 'lotes: :ounting Uncertainty is calculated at the 68% confidence level (I-sigma). ;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is he greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 15 of 18 SDG: 514075 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps & Springs 2020 Lab Sample ID: 2006528-005 Client Sample ID: Back Spring ANAl'Vf tC A I I AO O RATORIFS Collection Date: 6/16/2020 945h Received Date: 6/18/2020 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84119 Arsenic mg/L 6/19/2020 1313h 7/1/2020 1336h E200.8 0.00500 < 0.00500 Beryllium mg/L 6/19/2020 1313h 7/1/2020 1402h E200.8 0.000500 < 0.000500 Cadmium mg/L 6/19/2020 1313h 7/1/2020 1336h E200.8 0.000500 < 0.000500 Phone: (801)263-8686 Calcium mg/L 6/19/2020 1313h 7/1/2020 1921h E200.7 10.0 124 Chromium mg/L 6/19/2020 1313h 7 /I /2020 1336h E200.8 0.0250 < 0.0250 foll Free: (888) 263-8686 Cobalt mg/L 6/19/2020 13 13h 7/1/2020 1336h E200.8 0.0100 < 0.0100 Fax: (801) 263-8687 Copper mg/L 6/19/2020 1313h 7/1/2020 1336h E200.8 0.0100 < 0.0100 !-mail: awal@awal-labs.com Iron mg/L 6/19/2020 1313h 7 / l/2020 1402h E200.8 0.0300 < 0.0300 Lead mg/L 6/19/2020 1313h 7/1/2020 1402h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 6/19/2020 1313h 7/1/2020 1921 h E200.7 10.0 33.7 Manganese mg/L 6/19/2020 1313h 7/1/2020 1336h E200.8 0.0100 < 0.0100 Mercury mg/L 6/24/2020 1313h 6/25/2020 932h E245.l 0.000500 < 0.000500 Kyle F. Gross Molybdenum mg/L 6/19/2020 l 3 l 3h 7/1/2020 1336h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 6/19/2020 13 13h 7/1/2020 1336h E200.8 0.0200 < 0.0200 Potassium mg/L 6/19/2020 1313h 7/3/2020 1214h E200.7 1.00 7.23 Jose Rocha Selenium mg/L 6/19/2020 131 Jh 7/1/2020 1336h E200.8 0.00500 < 0.00500 QA Officer Silver mg/L 6/19/2020 1313h 7/1/2020 1336h E200.8 0.0100 < 0.0100 Sodium mg/L 6/19/2020 1313h 7/1/2020 1921h E200.7 10.0 282 Thallium mg/L 6/19/2020 1313h 7/1/2020 1402h E200.8 0.000500 < 0.000500 Tin mg/L 6/19/2020 1313h 7 /I /2020 1336h E200.8 0.100 <0.100 Uranium mg/L 6/19/2020 131 3h 7/1 /2020 1436h E200.8 0.000300 0.0107 Vanadium mg/L 6/19/2020 1313h 7/3/2020 1214h E200.7 0.0150 < 0.0150 Zinc mg/L 6/19/2020 1313h 7/1/2020 1336h E200.8 0.0100 <0.0100 Report Date: 7/6/2020 Page IO of 38 All anal~ ses api,licable to [he CWA. SDWA. and RCRA are perfom1ed in accordance Lo NELAC protocols Pertinent sampling inrormalion is localed on Lhe attached COC Confidential Business Information: This report is provided for1he exclusive use of the ~ddressee Pri, ile~es o! sub.seq~nl .~e of Lhe ~~e of this _con:1pany or an~ ~mber of its staJI or reproductio~ ~f Lhis repo~ in ~~eel ion~ \Vilh the ~:ertise~en(.. P~?moli~ or saJe of~~: ~rod~cl or p~ocess, ~r in 7onn:c!ion w!lh lh~ r:-publication of this report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps & Springs 2020 Lab Sample ID: 2006528-005 Client Sample ID: Back Spring t.H AI 'fTICA I I An011.AT0 Rlt:S Collection Date: 6/16/2020 945h Received Date: 6/18/2020 l lOOh Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual falt Lake City, UT 84119 Ammonia (as N) mg/L 6/25/2020 1035h 6/25/2020 2058h E350.1 0.0500 < 0.0500 Bicarbonate (as mg/L 6/19/2020 808h SM2320B 1.00 284 CaC03) Carbonate (as CaC03) mg/L 6/19/2020 808h SM2320B 1.00 < 1.00 Phone: (801)263-8686 Chloride mg/L 6/25/2020 2123h E300.0 5.00 147 Toll Free: (888) 263-8686 Fluoride mg/L 6/25/2020 2230h E300.0 0.100 0.240 Fax: (80 I) 263-8687 Ion Balance % 7/2/2020 858h Cale. -100 6.85 !-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 6/25/2020 t 249h E353.2 0.100 <0.100 Sulfate mg/L 6/25/2020 2123h E300.0 37.5 424 web: www.awal-labs.com Total Anions, Measured meq/L 7/2/2020 858h Cale. 18.7 Total Cations, meq/L 7/2/2020 858h Cale. 21.4 Measured Total Dissolved Solids mg/L 6/19/2020 t 209h SM2540C 20.0 1,280 Kyle F. Gross Total Dissolved Solids Cale. 1.07 7/2/2020 858h Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 7/2/2020 858h Cale. 1,190 Calculated QA Officer Report Date: 7/6/2020 Page 15 of38 All analyses applicable lo the CWA. SOWA. and RCRA are performed m accordance lo NELAC prolocols Pertinenl sampling information is located on the allad1ed COC Conlidential Business Information: This report is provided for lhe exclusi\ e use oflhe ~ddressee Pri, ile~es o~ sub .. seq~ent .u!e or lhe ~~e or this .con.1pany or an~· ~mber of iLs staff or reproduclio~ ~f lhis repo~ in ~on'.1eclion~ \dth lhe .,~, ertisement. P~?mo1io0n or sale of~!) ~rod~cl or p~ocess, ~r in ~onn~c~ion "~th th~ r~-publicalion of this report 3440 South 700 West ,alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Annual Seeps & Springs 2020 2006528-005A Client Sample ID: Back Spring Collection Date: 6/16/2020 945h Received Date: 6/18/2020 1100h Analytical Results Analyzed: 6/19/2020 910h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chlorofonn Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Extracted: Dilution Factor: Contact: Tanner Holliday Test Code: 82600-W-DENlOO VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount piked %REC Limits Qual Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 47.3 52.1 46.7 52.9 50.00 94.6 72-151 50.00 104 80-152 50.00 93.3 72-135 50.00 106 80-124 Report Date: 7/6/2020 Page 20 of38 All analyses applicable lo lhe CWA. SDWA, and RCRA are perfonned in accordance lo NE LAC prolocols Pertinent sampling informalion is located on the altached COC. Confidential Business Information: This report is pro,·ided for lhe exclusive use of the ~ddressee Pri \ ilc~es o_f sub__seq~enl ~e of the ~~e of I his .con_1pany or any ~mber of its stllff, or reproducli~ ~f I his repo~ in ~on~ection" with the ~,,ertisemenl, P~?molio.n or saJe of~~ ~rod~ct or p~ocess, ~r in ~onn:'~ion ,,·~th lh~ r:-publicalion of lhis report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: July I 3, 2020 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: Analytical for Annual Seeps & Springs 2020 -------Client Sample ID: Back Spring Sample ID: 514075005 Matrix: Ground Water Collect Date: 16-JUN-20 09:45 Receive Date: l 9-JUN-20 Collector: Client Parameter Qualifier Result Uncertainty lad Gas Flow Proportional Counting ]FPC, Total Alpha Radium, Liquid "As Received" ,ross Radium Alpha U -0.00212 +/-0.191 The following Analytical Methods were performed: \1ethod Descri tion EPA 903.0 Test MDC 0.739 ~rrogate/Tracer Recovery 3arium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 1fotes: :ounting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 ---~------------- Project: Client ID: DNMI00106 DNMIOOI Units PF OF Analyst Date Time Batch Method pCi/L JXK3 07/01/20 1247 2013767 Result Analvst Comments Nominal Recovery% 95.9 Acceptable Limits (25%-125%) iRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is he greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 16 of 18 SDG: 514075 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit 3440 South 700 West ,alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Annual Seeps & Springs 2020 2003627-002A Client Sample ID: Trip Blank Collection Date: 3/25/2020 1300h Received Date: 3/27/2020 1100h Analytical Results Analyzed: 3/27/2020 1418h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surrogate Units: µg/L Surr: l ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Extracted: Dilution Factor: CAS 17060-07-0 460-00-4 1868-53-7 2037-26-5 1 Contact: Tanner Holliday Test Code: 82600-W-DENlOO VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Result Amount Spiked %REC Limits Qual 53.0 50.00 106 72-151 50.8 50.00 102 80-152 49.0 50.00 98.0 72-135 49.3 50.00 98.6 80-124 Report Date: 4/10/2020 Page 8 of26 All analyses applicable lo lhe CWA. SOWA. and RCRA nre perfo,rned in accordance 10 NELAC protocols_ Pertinenl sampling information is localed on the attnched COC Confidenlial Business Jnfonnotion: This repon is pro\•ided for lhe e.~clush e use of lhe ~ddressee Prhile~es o.fsub,_seq~nl ~;e of lhe ~?':'1e of this .con;ipany or nnr ~mber of its st:irT, or reproducli~ ~~this repo~ in .c~teclion .. "~lh the a~vertise~nt, P~?motio.n ~r ~ale of~!Y ~rod~cl or pi:ocess, ~r in 7°nn~c!ion "'!'h th~ r~-p~blication of I.his report /INo\t'W f lCA( I Afl ORAJOJJ IEi 3440 South 700 West ,alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, [nc. Annual Seeps & Springs 2020 2006528-006A Client Sample ID: Trip Blank Collection Date: 6/16/2020 Received Date: 6/18/2020 Analytical Results Analyzed: 6/19/2020 930h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surrogate Units: µg/L Surr: l ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 845h 1100h Extracted: Dilution Factor: CAS 17060-07-0 460-00-4 1868-53-7 2037-26-5 Contact: Tanner Holliday Test Code: 8260D-W-DEN100 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qua! 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 3.83 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Result Amount Spiked %REC Limits Qual 48.0 50.00 96.1 72-151 53.1 50.00 106 80-152 46.1 50.00 92.3 72-135 52.8 50.00 106 80-124 Report Date: 7/6/2020 Page 21 of38 All anal)ses applicable lo lhe CWA, SDWA. and RCRA are perfom1ed in accordance to NELAC protocols. Per1inent sampling inrormaLion is located on the allached COC, Confidential Business lnformulion: This report is pr°' ided for lhe excJUSi\ e use of !he ~ddressee. Pri\ ile~es of sub.5eq~enl ~e of the ~~e of this _co~pnn~· or anr ~mber of its staIT. or reproduclio~ ~~ Lhis repo~ in .con~1ection~ wilh the~' ertisemenL p~~motio.n or saJe of :u!Y ~rod~ct or p~ocess, ~r in ~onn:c~ion w~lh th~ r:-publication of this report 3440 South 700 West ;alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Tanner Holliday Energy Fuels Resources, Inc. 6425 South Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: Annual Seeps & Springs 2020 Dear Tanner Holliday: Lab Set ID: 2003627 American West Analytical Laboratories received sample(s) on 3/27/2020 for the analyses presented in the following report. American West Analytical Laboratories (AWAL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, Wyoming, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Digitally signed by Jose G. J OS e G ~~~~~=Jose G. Rocha, • o=American West Analytical Laboratories, ou=UT00031, RO Ch a ~:itjose@awal-labs.com, Date: 2020.04.10 16:38:50 Approved by: -os·oo· Laboratory Director or designee Report Date: 4/10/2020 Page I of 26 All analyses applicable to lhe CW A. SOWA and RCRA are perfom1ed in accordance lo NELAC protocols. Pertinen1 sampling information is localed on lhe attached COC. (lf1tidi:nliul Business Informal ion: This report is provided for the bS.Clt~\"'<! I.do of the !ddressee Pri,-ile~es o! su~seq~t ~;e of the ~~ne of this .con:ipany or M) ~mbei of its s1arr, or reproducli~ ~~this repo~ in ~on~eclion~ ,vilh the a~Yertise~nl, P~?moliO:,' ~r~c: or?'~: ~rod~ct or P~?Cess, ~r in ~nn~c!ion w!th th~ r~-p~blicntlan of lhis reporl American West Client: ANALYTICAL lABORATORIE6 Project: Lab Set ID: Date Received: Lab Sample ID 3440 South 700 West 2003627-00IA ,alt Lake City, UT 84119 2003627-0018 2003627-0018 Phone: (801)263-8686 2003627-00lC Toll Free: (888) 263-8686 2003627-00JD Fax:(801)263-8687 2003627-001 D :-mail : awal@awal-labs.com 2003627-00IE web: www.awal-labs.com 2003627-00 IE 2003627-00lE 2003627-00IE Kyle F. Gross 2003627-002A Laboratory Director Jose Rocha QA Officer SAMPLE SUMMARY Energy Fuels Resources, Inc. Annual Seeps & Springs 2020 2003627 Contact: Tanner Holliday 3/27/2020 1100h Client Sample ID Date Collected Matrix Analysis Westwater Spring 3/25/2020 1300h Aqueous VOA by GC/MS Method 8260D/5030C Westwater Spring 3/25/2020 1300h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level Westwater Spring 3/25/2020 1300h Aqueous Anions, E300.0 Westwater Spring 3/25/2020 1300h Aqueous Total Dissolved Solids, A2540C Westwater Spring 3/25/2020 1300h Aqueous Ammonia, Aqueous Westwater Spring 3/25/2020 1300h Aqueous Nitrite/Nitrate (as N), E353.2 Westwater Spring 3/25 /2020 1300h Aqueous Mercury, Drinking Water Dissolved Westwater Spring 3/25/2020 1300h Aqueous ICPMS Metals, Dissolved Westwater Spring 3/25/2020 1300h Aqueous ICP Metals, Dissolved Westwater Spring 3/25/2020 1300h Aqueous Ion Balance Trip Blank 3/25/2020 1300h Aqueous VOA by GC/MS Method 8260D/5030C Report Date: 4/10/2020 Page 2 of 26 All analyses applicable to lhe CWA. SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling informiltion is Jocuted on lhe attached COC. Confidentiol Business Jnformation: This repon is prO\•ided for the e.xclush e use of the ~ddressee Pri\ ile~es of sub .. seq~enl ~~e or the ~?':"e of this .con_ipany or nn} ~';'ber or its slaff, or reproducti~ ~f this repo~ in ~on~lection .. v.,i1h lhe o~,•enisement, P~?motio.n ~r ~aJe of~!)~ ~rod~cl or P~?cess, ~r in ~nn:_c~ion w!lh th~ r~-publicruion of this repon American West ANALYTICAL LABORATORIES 3440 South 700 West ;alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: Annual Seeps & Springs 2020 2003627 3/27/2020 3/25/2020 Intact None Holding Time and Preservation Requirements: The analysis and preparation of all samples were performed within the method holding times. All samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPO: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in contr?l. Matrix Spike / Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exception: the MS percent recovery, MSD percent recovery, and RPO for Ammonia on sample 2003627-001 were outside of the control limits due to sample non-homogeneity and/or sample matrix interference. Duplicate (DUP): The RPO for Total Dissolved Solids on sample 2003627-001 was outside of the control limits due to sample non-homogeneity or sample matrix interference. Corrective Action: None required. Report Date: 4/10/2020 Page 3 of 26 All anal)ses applicable to lhe CWA SOWA, and RCRA are perfomied in accordance to NELAC protocols Pertinenl sampling infonnation is located on the etlached COC Confidential Business lnfonno1ion: This reporl is pro,ided ror 1he exclusi, e use 0C1he ~ddressee Pri,·ile~es o_r sub,_seq~eni ~~e or the ~~e of this .co1~pany or MY ~mber of its staff, or reproductio~ ~f this repo~ in fOl~eclioo .. "~th the a~vertisement. p~~motio,n ~r saJe of~!~: ~rodl~l or p~~cess, ~r in ~nn~~ion w!th lh~ r~-publication of lhis report American West ANALYTICAL LAB0RAT0Rlf6 3440 South 700 West ~alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: Method: Analysis: Annual Seeps & Springs 2020 2003627 3/27/2020 3/25/2020 Intact None SW-846 8260D/5030C Volatile Organic Compounds General Set Comments: No target analytes were observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met, with CCV exceptions noted on the reports. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike / Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 4/10/2020 Page 4 of 26 All annlyses applicable to the CWA. SOWA. and RCRA nre perfonned in accordance to NELAC protocols. Peninenl sampJin1:, informa1ion is located on the attached COC. Confidenlial Business Jnformation: This repon is pro,•ided for the exclusi, e use of the ~ddressec Privile~es o_f sub .. seq~enl ~1;e of the ~~e of !his .co"?pony or nnr ~mber of its s13IT, or reproduclio~ ~f this repo~ in .con?eclion .. \\~th the n~, ertisemenl, P~?moli~ or sale of?'!): ~rod~ct or p~ocess, ~r in ~onn~c!ion w(th lh~ r~-publication of this report 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer ANALYTICAL LABORATORIES , C SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2003627 Dept: ME Project: Annual Seeps & Springs 2020 QC Type: LCS -~- Reporting Amount Spiked Spike Ref. RPO Ref. RPO Analyte Result Units Method MDL Limit Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: LCS-69049 Date Analyzed: 04/06/2020 1518h Test Code: 200.7-DIS Date Prepared: 04/05/2020 l 039h Calcium 9.89 mg/L E200.7 0.211 1.00 10.00 0 98.9 85 -115 Magnesium 10.4 mg/L E200.7 0.0654 1.00 10.00 0 104 85 -115 Potassium 10.6 mg/L E200.7 0.246 1.00 10.00 0 106 85 -115 Sodium 10.5 mg/L E200.7 0.123 1.00 10.00 0 105 85 -115 Lab Sample ID: LCS-69050 Date Analyzed: 04/07/2020 1333h Test Code: 200.8-DIS Date Prepared: 04/05/2020 1039h Arsenic 0.200 mg/L E200.8 0.000298 0.00200 0.2000 0 100 85 -115 Beryllium 0.203 mg/L E200.8 0.000198 0.00200 0.2000 0 101 85 -115 Cadmium 0.201 mg/L E200.8 0.0000742 0.000500 0.2000 0 100 85 -115 Chromium 0.197 mg/L E200.8 0.00191 0.00200 0.2000 0 98.4 85 -115 Cobalt 0.203 mg/L E200.8 0.000300 0.00400 0.2000 0 101 85 -115 Copper 0.199 mg/L E200.8 0.00166 0.00200 0.2000 0 99.3 85 -115 Iron 0.984 mg/L E200.8 0.0328 0.100 1.000 0 98.4 85 -115 Lead 0.200 mg/L E200.8 0.000448 0.00200 0.2000 0 JOO 85 -115 Manganese 0.197 mg/L E200.8 0.000766 0.00200 0.2000 0 98.3 85 -115 Molybdenum 0.204 mg/L E200 8 0.000652 0.00200 0.2000 0 102 85 -115 Nickel 0.200 mg/L E200.8 0.000728 0.00200 0.2000 0 99.8 85 -115 Selenium 0.192 mg/L E200,8 0.000508 0.00200 0.2000 0 95.9 85 -115 Silver 0.201 mg/L E200.8 0.000232 0.00200 0.2000 0 100 85 -115 Thallium 0.198 mg/L E200.8 0.000390 0.00200 0.2000 0 99.0 85 -115 Tin 1.03 mg/L E200,8 0.00115 0.00400 1.000 0 103 85 -115 Uranium 0.214 mg/L E200,8 0.000176 0.00200 0.2000 0 107 85 -115 Zinc 0.982 mg/L E200,8 0.00418 0.00600 1.000 0 98.2 85 -115 Lab Sample ID: LCS-69050 Date Analyzed: 04/08/2020 1252h Test Code: 200.8-DIS Date Prepared: 04/05/2020 1039h Vanadium 0.208 mg/L E200.8 0.00152 0.00440 0.2000 0 104 85 -115 Report Date: 4/10/2020 Page 9 of26 analyses applicable to the CWA. SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement_ promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This Client: Energy Fuels Resources, Inc. Lab Set ID: 2003627 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: LCS-68916 Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury 0.00358 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Tanner Holliday Dept: ME QC Type: LCS Reporting Amount Spiked Spike Ref. Method MDL Limit Amount %REC 03/30/2020 IOO!h 03/27/2020 1335h mg/L E245.I 0.0000396 0.0000900 0.003330 0 107 Limits 85 -115 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 4/10/2020 Page IO of 26 analyses applicable to the CW A. SDW A, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC Confidential Business lnfonnation: This report is provided for the exclusive use of the addressee Privile<>,,es of subsequent use of It ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This American West APULYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2003627 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: MB-69049 Date Analyzed: Test Code: 200.7-DIS Date Prepared: Calcium < 1.00 Magnesium < l.00 Potassium < 1.00 Sodium < l.00 Lab Sample ID: MB-FIL TER-68854 Date Analyzed: Test Code: 200.7-DJS Date Prepared: Calcium < l.00 Magnesium < l.00 Potassium < 1.00 Sodium < 1.00 Lab Sample ID: MB-69050 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Beryllium < 0.000200 Iron < 0.0100 Lead < 0.000200 Thallium < 0.000200 Uranium < 0.000200 Lab Sample ID: MB-69050 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Arsenic < 0.00200 Cadmium < 0.000500 Chromium < 0.00200 Cobalt < 0.00400 Copper < 0.00200 Manganese < 0.00200 Molybdenum < 0.00200 3440 South 700 West Salt Lake City, UT 841 I 9 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Units Method MDL Limit 04/06/2020 1515h 04/05/2020 1039h mg/L E200.7 0.211 1.00 mg/L E200.7 0.0654 1.00 mg/L E200.7 0.246 1.00 mg/L E200.7 0.123 1.00 04/06/2020 1536h 04/05/2020 I 039h mg/L E200.7 0.211 1.00 mg/L E200.7 0.0654 1.00 mg/L E200.7 0.246 1.00 mg/L E200.7 0.123 1.00 04/07/2020 1327h 04/05/2020 1039h mg/L E200.8 0.0000198 0.000200 mg/L E200 8 0.00328 0.0100 mg/L E200.8 0.0000448 0.000200 mg/L E200.8 0.0000390 0.000200 mg/L E200.8 0.0000176 0.000200 04/07/2020 1330h 04/05/2020 1039h mg/L E200.8 0.000298 0.00200 mg/L E200.8 0.0000742 0.000500 mg/L E200.8 0.00191 0.00200 mg/L E200.8 0.000300 0.00400 mg/L E200.8 0.00166 0.00200 mg/L E200.8 0.000766 0.00200 mg/L E200.8 0.000652 0.00200 Tanner Holliday ME MBLK Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 4/10/2020 Page 11 of26 analyses applicable to the CWA. SOWA, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee Priv~eges of subsequent use of ti- ne of this company or any member of its staff. or reproduction of this report in connection with the advertisement,. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact.. This ANALYTIC AL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2003627 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: MB-69050 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Nickel < 0.00200 Selenium < 0.00200 Silver < 0.00200 Tin < 0.00400 Zinc < 0.00600 Lab Sample ID: MB-FIL TER-68854 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Arsenic < 0.00200 Beryllium < 0.00200 Cadmium < 0.000500 Chromium < 0.00200 Cobalt < 0.00400 Copper < 0.00200 Iron < 0.100 Lead < 0.00200 Manganese < 0.00200 Molybdenum < 0.00200 Nickel < 0.00200 Selenium < 0.00200 Silver < 0.00200 Thallium < 0.00200 Tin < 0.00400 Uranium < 0.00200 Zinc < 0.00600 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Units Method MDL Limit 04/07/2020 1330h 04/05/2020 1039h mg/L E200.8 0.000728 0.00200 mg/L E200.8 0.000508 0.00200 mg/L E200.8 0.000232 0.00200 mg/L E200.8 0.00115 0.00400 mg/L E200.8 0.00418 0.00600 04/07/2020 1343h 04/05/2020 1039h mg/L E200.8 0.000298 0.00200 mg/L E200.8 0.000198 0.00200 mg/L E200.8 0.0000742 0.000500 mg/L E200.8 0.00191 0.00200 mg/L E200.8 0.000300 0.00400 mg/L E200.8 0.00166 0.00200 mg/L E200 8 0.0328 0.100 mg/L E200,8 0.000448 0.00200 mg/L E200.8 0.000766 0.00200 mg/L E200.8 0.000652 0.00200 mg/L E200.8 0.000728 0.00200 mg/L E200.8 0.000508 0.00200 mg/L E200.8 0.000232 0.00200 mg/L E200.8 0.000390 0.00200 mg/L E200 8 0.00115 0.00400 mg/L E200.8 0.000176 0.00200 mg/L E200.8 0.00418 0.00600 Tanner Holliday ME MBLK Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit Qual Report Date: 4/10/2020 Page 12 of26 analyses applicable to the CWA. SDW A, and RCRA are perfonned in accordance to NELAC protocols Pertinent sampling information is located on the attached COC. Confidential Business information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This Client: Energy Fuels Resources, Inc. Lab Set ID: 2003627 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: MB-FILTER-69023 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Arsenic < 0.00200 Lab Sample ID: MB-69050 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Vanadium < 0.00440 Lab Sample ID: MB-FILTER-68854 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Vanadium < 0.00440 Lab Sample ID: MB-68916 Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury < 0.0000900 3440 South 700 West Salt Lake City, UT 84 I I 9 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Units Method MDL Limit 04/07/2020 1426h 04/05/2020 1039h mg/L E200.8 0.000298 0.00200 04/08/2020 1248h 04/05/2020 1039h mg/L E200.8 0.00152 0.00440 04/08/2020 1308h 04/05/2020 1039h mg/L E200.8 0.00152 0.00440 03/30/2020 959h 03/27/2020 1335h mg/L E245.l 0.0000396 0.0000900 Tanner Holliday ME MBLK Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPO Limit Qual Report Date: 4/10/2020 Page 13 of26 analyses applicable to the CWA. SOWA, aod RCRA are perl"onned in accordance to N ELAC protocols. Pertinent sampling infonnation is located on the attached COC. Confidential Business lnfonnation: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of tt ne of this company or any member of its staff~ or reproduction of this report io connection with the advertisement:,. promotion or sale of any product or process~ or in connection with the re-publication of this report for any purpose other than for the addressee wi11 be granted only on contact. This 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer Al>IALYTICAL LABORATORIES ""C SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2003627 Dept: ME Project: Annual Seeps & Springs 2020 QC Type: MS Reporting Amount Spiked Spike Ref. RPDRef. RPO Analyte Result Units Method MDL Limit Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 2003627-00IEMS Date Analyzed: 04/06/2020 1530h Test Code: 200.7-DIS Date Prepared: 04/05/2020 1039h Calcium 213 mg/L E200.7 2.11 10.0 100.0 118 94.3 70 -130 Magnesium 137 mg/L E200,7 0.654 10.0 100.0 30.8 106 70 -130 Potassium 110 mg/L E200,7 2.46 10.0 100.0 0 110 70 -130 Sodium 218 mg/L E200.7 1.23 10.0 100.0 117 101 70 -130 Lab Sample ID: 2003627-00IEMS Date Analyzed: 04/07/2020 1615h Test Code: 200.8-DIS Date Prepared: 04/05/2020 I 039h Arsenic 1.95 mg/L E200.8 0.00298 0.0200 2.000 0.00137 97.2 75 -125 Beryllium 2.01 mg/L E200.8 0.00198 0.0200 2.000 0 100 75 -125 Cadmium 1.99 mg/L E200.8 0.000742 0.00500 2.000 0 99.7 75 -125 Chromium 2.01 mg/L E200.8 0.0191 0.0200 2.000 0 101 75 -125 Cobalt 2.06 mg/L E200.8 0.00300 0.0400 2.000 0.000745 103 75 -125 Copper 2.02 mg/L E200.8 0.0166 0.0200 2.000 0 101 75 -125 Iron 10.4 mg/L E200.8 0.328 1.00 10.00 0.401 99.8 75 -125 Lead 1.99 mg/L E200 8 0.00448 0.0200 2.000 0 99.4 75 -125 Manganese 2.31 mg/L E200.8 0.00766 0.0200 2.000 0.369 97.1 75 -125 Molybdenum 2.06 mg/L E200,8 0.00652 0.0200 2.000 0.00177 103 75 -125 Nickel 2.06 mg/L E200.8 0.00728 0.0200 2.000 0 103 75 -125 Selenium 1.91 mg/L E200.8 0.00508 0.0200 2.000 0 95.5 75 -125 Silver 1.97 mg/L E200.8 0.00232 0.0200 2.000 0 98.4 75 -125 Thallium 2.01 mg/L E200.8 0.00390 0.0200 2.000 0 100 75 -125 Tin 10.7 mg/L E200.8 0.0115 0.0400 10.00 0 107 75 -125 Uranium 2.13 mg/L E200.8 0.00176 0.0200 2.000 0.00234 106 75 -125 Vanadium 2.03 mg/L E200.8 0.0152 0.0440 2.000 0 102 75 -125 Zinc 9.88 mg/L E200.8 0.0418 0.0600 10.00 0 98.8 75 -125 Report Date: 4/10/2020 Page 14 of 26 analyses applicable to the CWA. SDWA, and RCRA are performed in accor<lance to NELAC protocols. Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee. Privileges of subsequent use oft~ ne ofthjs company or any member of its staff~ or reprochJction of this report in connection with the advertisement, promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other-than for the addressee will be granted only on contact. This Client: Energy Fuels Resources, Inc. Lab Set ID: 2003627 Project: Annual Seeps & Springs 2020 Analyte Result Units 3440 South 700 West Salt Lake City, UT 84 I I 9 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Tanner Holliday Dept: ME Method MDL Reporting Limit QCType: MS Amount Spiked Spike Ref. Amount %REC Lab Sample ID: 2003627-00IEMS Test Code: HG-DW-DIS-245.1 Date Analyzed: 03/30/2020 IOI Oh Date Prepared: 03/27/2020 1335h Mercury 0.00342 mg/L E245.l 0.0000396 0.0000900 0.003330 0 103 Limits 85 -115 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Limit Amt %RPD Qual Report Date: 4/10/2020 Page 15 of26 analyses applicable to the CWA, SOWA, and RCRA are perfonned in accordance to NELAC protocols Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee. Privileges of subsequent use oftt ne of this company or any member of its staff~ or reproduction of this report in connection with the advertisement promotion or sa1e of any product or process~ or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West QC SUMMARY REPORT ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2003627 Dept: ME Project: Annual Seeps & Springs 2020 QC Type: MSD Reporting Amount Spiked Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Amount %REC Limits Amt %RPD Limit Qual Lab Sample ID: 2003627-00IEMSD Date Analyzed: 04/06/2020 1533h Test Code: 200.7-DIS Date Prepared: 04/05/2020 1039h Calcium 201 mg/L E200.7 2.11 10.0 100.0 118 83.0 70 -130 213 5.45 20 Magnesium 130 mg/L E200.7 0.654 10.0 100.0 30.8 99.6 70 -130 137 4.71 20 Potassium 110 mg/L E200 7 2.46 10.0 100.0 0 110 70 -130 110 0.124 20 Sodium 207 mg/L E200.7 1.23 10.0 100.0 117 89.4 70 -130 218 5.34 20 Lab Sample ID: 2003627-00IEMSD Date Analyzed: 04/07/2020 1618h Test Code: 200.8-DIS Date Prepared: 04/05/2020 1039h Arsenic 1.96 mg/L E200,8 0.00298 0.0200 2.000 0.00137 98.1 75 -125 1.95 0.944 20 Beryllium 2.03 mg/L E200.8 0.00198 0.0200 2.000 0 IOI 75 -125 2.01 1.16 20 Cadmium 1.99 mg/L E200,8 0.000742 0.00500 2.000 0 99.7 75 -125 1.99 0.0411 20 Chromium 1.99 mg/L E200.8 0.0191 0.0200 2.000 0 99.6 75 -125 2.01 0.888 20 Cobalt 2.05 mg/L E200.8 0.00300 0.0400 2.000 0.000745 102 75 -125 2.06 0.395 20 Copper 2.03 mg/L E200.8 0.0166 0.0200 2.000 0 101 75 -125 2.02 0.142 20 Iron 10.3 mg/L E200.8 0.328 1.00 10.00 0.401 99.3 75 -125 10.4 0.458 20 Lead 2.02 mg/L E200.8 0.00448 0.0200 2.000 0 101 75 -125 1.99 1.42 20 Manganese 2.34 mg/L E200.8 0.00766 0.0200 2.000 0.369 98.6 75 -125 2.31 1.32 20 Molybdenum 2.03 mg/L E200.8 0.00652 0.0200 2.000 0.00177 101 75 -125 2.06 1.81 20 Nickel 2.04 mg/L E200.8 0.00728 0.0200 2.000 0 102 75 -125 2.06 0.979 20 Selenium 1.90 mg/L E200,8 0.00508 0.0200 2.000 0 95.1 75 -125 1.91 0.415 20 Silver 1.98 mg/L E200.8 0.00232 0.0200 2.000 0 99.1 75 -125 1.97 0.797 20 Thallium 1.98 mg/L E200.8 0.00390 0.0200 2.000 0 99.0 75 -125 2.01 1.45 20 Tin 10.3 mg/L E200.8 0.0115 0.0400 10.00 0 103 75 -125 10.7 4.09 20 Uranium 2.16 mg/L E200 8 0.00176 0.0200 2.000 0.00234 108 75 -125 2.13 1.40 20 Vanadium 2.03 mg/L E200,8 0.0152 0.0440 2.000 0 102 75 -125 2.03 0.00256 20 Zinc 9.99 mg/L E200.8 0.0418 0.0600 10.00 0 99.9 75 -125 9.88 1.09 20 Report Date: 4/10/2020 Page 16 of26 analyses applicable to the CWA, SOWA, and RCRA are performed in accordance to NELAC protocols, Pertinent sampling information is located on the attached COC. Confidential Business Information: TI1is report is provided for the exclusive use of the addressee. Privileges of subsequent use of ti- ne of this company or any member of its staff~ or reproduction of this report in connection with the advertisement. promotion or sa1e of any product or process. or in connection with the re-publication of this report for any pwpose other than for the addressee wi11 be granted only on contact This Client: Energy Fuels Resources, Inc. Lab Set ID: 2003627 Project: Annual Seeps & Springs 2020 Analyte Result Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-Iabs.com C SUMMARY REPORT Contact: Dept: Tanner Holliday ME Method MDL Reporting Limit QC Type: MSD Amount Spiked Spike Ref. Amount %REC Lab Sample ID: 2003627-00IEMSD Test Code: HG-DW-DIS-245.l Date Analyzed: 03/30/2020 1012h Date Prepared: 03/27/2020 1335h Mercury 0.00342 mg/L E245.l 0.0000396 0.0000900 0.003330 0 103 Limits 85 -115 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. Amt %RPO 0.00342 0.0487 RPD Limit 20 Qual Report Date: 4/10/2020 Page 17 of26 analyses applicable to the CWA, SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. Confidential Business Information: This repon is provided for the exclusive use of the addressee. Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, oc in connection with the re-publication of this report for any purpose other than for the addressee will be granted only oo conlaet. This Client: Energy Fuels Resources, Inc. Lab Set ID: 2003627 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: 2003627-001 CDUP Date Analyzed: Test Code: TDS-W-2540C Total Dissolved Solids 1,070 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Method MDL Limit Tanner Holliday WC DUP Spike Ref. Amount %REC 03/30/2020 1140h mg/L SM2540C 16.0 20.0 @ -High RPD due to suspected sample non-homogeneity or matrix interference. Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPO Limit 1200 11.3 5 Qual @ Report Date: 4/10/2020 Page 18 of26 analyses applicable to the CWA, SDW A, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisemenl promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2003627 Project: Annual Seeps & Springs 2020 Analyte Result Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 I) 263-8686, Toll Free: ( 888) 263-8686, Fax: ( 801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Tanner Holliday Dept: WC Method MDL Reporting Limit QCType: LCS Amount Spiked Spike Ref. Amount %REC Lab Sample ID: LCS-Rl37196 Date Analyzed: 03/31/2020 2344h Test Code: 300.0-W Chloride Fluoride Sulfate Lab Sample ID: LCS-R137118 Test Code: ALK-W-2320B-LL Alkalinity (as CaC03) Lab Sample ID: LCS-68969 Test Code: NH3-W-350.l Ammonia (as N) Lab Sample ID: LCS-Rl37224 Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) Lab Sample ID: LCS-R137131 Test Code: TDS-W-2540C Total Dissolved Solids 5.12 mg/L E300.0 5.09 mg/L E300,0 5.05 mg/L E300.0 Date Analyzed: 03/31/2020 729h 250 mg/L SM2320B Date Analyzed: 04/02/2020 1441h Date Prepared: 04/01/2020 846h 1.85 mg/L E350.l -Date Analyzed: 04/02/2020 1022h 1.10 mg/L E353,2 Date Analyzed: 03/30/2020 1140h 208 mg/L SM2540C 0.0565 0.100 0.0240 0.100 0.136 0.750 0.369 1.00 0.0473 0.0500 0.00494 0.0100 8.00 10.0 5.000 5.000 5.000 250.0 2.000 1.000 205.0 0 0 0 0 0 0 0 102 102 101 100 92.4 llO IOI Limits 90 -110 90 -110 90 -110 90 -110 90 -110 90 -110 80 -120 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Limit Amt %RPO Qual Report Date: 4/1 0/2020 Page 19 of 26 analyses applicable to the CW A, SDW A, and RCRA are performed in accordance to NE LAC protocols Pertinent sampling infom1ation is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee wil1 be granted only on contact. This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2003627 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: MB-R137196 Date Analyzed: Test Code: 300.0-W Chloride < 0.100 Fluoride <0.100 Sulfate < 0.750 Lab Sample ID: MB-RI37118 Date Analyzed: Test Code: ALK-W-23208-LL Bicarbonate (as CaC03) < 1.00 Carbonate (as CaC03) < 1.00 Lab Sample ID: MB-68969 Date Analyzed: Test Code: NH3-W-350.l Date Prepared: Ammonia (as N) < 0.0500 Lab Sample ID: MB-R137224 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) < 0.0100 Lab Sample ID: MB-R137131 Date Analyzed: Test Code: TDS-W-2540C Total Dissolved Solids < 10.0 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Units Method MDL Limit 03/31/2020 2327h mg/L E300.0 0.0565 0.100 mg/L E300.0 0.0240 0.100 mg/L E300.0 0.136 0.750 03/31/2020 729h mg/L SM2320B 0.369 1.00 mg/L SM2320B 0.369 1.00 04/02/2020 1408h 04/01/2020 846h mg/L E350.l 0.0473 0.0500 04/02/2020 1021h mg/L E353.2 0.00494 0.0100 03/30/2020 1140h mg/L SM2540C 8.00 10.0 Tanner Holliday WC MBLK Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPO Amt %RPO Limit Qual Report Date: 4/10/2020 Page 20 of 26 analyses applicable to the CWA. SOW A, and RCRA are performed in accordance to NE LAC protocols. Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of ti- ne of this company or any member of its staff, oc reproduction of this report in connection with the advertisement promotion or sa1e of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contacL This Client: Energy Fuels Resources, Inc. Lab Set ID: 2003627 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: 2003627-00IBMS Date Analyzed: Test Code: 300.0-W Chloride 273 Fluoride 256 Sulfate 544 Lab Sample ID: 2003627-00lBMS Date Analyzed: Test Code: ALK-W-2320B-LL Alkalinity (as CaC03) 366 Lab Sample ID: 2003627-00IDMS Date Analyzed: Test Code: NH3-W-350.l Date Prepared: Ammonia (as N) 1.73 Lab Sample ID: 2003627-00IDMS Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.08 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Units Method MDL Limit 04/01/2020 749h mg/L E300.0 2.82 5.00 250.0 mg/L E300.0 1.20 5.00 250.0 mg/L E300.0 6.80 37.5 250.0 03/31/2020 729h mg/L SM23208 0.369 1.00 100.0 04/02/2020 1432h 04/01/2020 846h mg/L E350.1 0.0473 0.0500 2.000 04/02/2020 1029h mg/L E353.2 0.00494 0.0100 1.000 Tanner Holliday WC MS Spike Ref. Amount %REC 26.6 98.4 0.555 102 307 94.5 270 96.0 0.0593 83.6 0.00555 107 1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Limits 90 -110 90 -110 90 -110 80 -120 90 -110 90 -110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPD Limit Qual Report Date: 4/10/2020 Page 21 of26 analyses applicable to the CWA. SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC. Confidential Business lnfomiation: T11is report is provided for the exclusive use of the addressee. Privileges of subsequent use of ti- ne of this company or any member of its staff. or reproduction of this report in connection with the advertisement,. promotion or sa1e of any product or process, or in connection with the re-publication of this report for any pwpose other than for the addressee wi11 be granted only on contact. This 3440 South 700 West Salt Lake City, UT 84 I I 9 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-Iabs.com, web: www.awal-labs.com Jose Rocha American West QA Officer _QC SUMMARY REPORT ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2003627 Dept: WC Project: Annual Seeps & Springs 2020 QC Type: MSD Reporting Amount Spiked Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 2003627-00IBMSD Date Analyzed: 04/01/2020 806h Test Code: 300.0-W Chloride 277 mg/L E300 0 2.82 5.00 250.0 26.6 100 90 -110 273 1.52 20 Fluoride 257 mg/L E300.0 1.20 5.00 250.0 0.555 103 90 -110 256 0.348 20 Sulfate 549 mg/L E300.0 6.80 37.5 250.0 307 96.9 90 -110 544 1.08 20 Lab Sample ID: 2003627-00IBMSD Date Analyzed: 03/31/2020 729h Test Code: ALK-W-23208-LL Alkalinity (as CaC03) 366 mg/L SM2320B 0.369 1.00 100.0 270 96.0 80 -120 366 0 10 Lab Sample ID: 2003627-00IDMSD Date Analyzed: 04/02/2020 1433h Test Code: NH3-W-350.l Date Prepared: 04/01/2020 846h Ammonia (as N) 1.42 mg/L E350.1 0.0473 0.0500 2.000 0.0593 67.8 90-110 1.73 20.0 IO '@ Lab Sample ID: 2003627-00IDMSD Date Analyzed: 04/02/2020 1030h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.03 mg/L E353.2 0.00494 0.0100 1.000 0.00555 102 90 -110 1.08 5.23 10 @ -High RPD due to suspected sample non-homogeneity or matrix interference. ' -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Report Date: 4/10/2020 Page 22 of26 analyses applicable to the CWA. SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC. Confidential Business Information: This repon is provided for the exclusive use of the addressee. Privileges of subsequent use oft~ ne of this company or any member of its staff~ or reproduction of this report in connection with the advertisement promotion or sa1e of any product or process~ or in connection with the re-publication of this report for any pwpose othcr than for the addressee will be granted only on contact. This Client: Energy Fuels Resources, Inc. Lab Set ID: 2003627 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: LCS VOC-1 0327208 Date Analyzed: Test Code: 8260D-W-DENIOO 2-Butanone 27.9 Acetone 37.5 Benzene 18.7 Carbon tetrachloride 18.8 Chloroform 19.5 Chloromethane 9.51 Methylene chloride 19.0 Naphthalene 18.3 Tetrahydrofuran 19.2 Toluene 18.0 Xylenes, Total 54.9 Surr: l ,2-Dichloroethane-d4 50.0 Surr: 4-Bromofluorobenzene 47.0 Surr: Dibromofluoromethane 48.5 Surr: Toluene-d8 47.5 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Method MDL Limit Tanner Holliday MSVOA LCS Spike Ref. Amount %REC 03/27/2020 1259h µg/L SW82600 1.22 20.0 20.00 0 139 µg/L SW82600 2.76 20.0 20.00 0 188 µg/L SW8260D 0.147 1.00 20.00 0 93.7 µg/L SW82600 0.859 1.00 20.00 0 93 .8 µg/L SW82600 0.166 1.00 20.00 0 97.6 µg/L SW8260D 0.802 1.00 20.00 0 47.6 µg/L SW8260D 0.381 1.00 20.00 0 95.2 µg/L SW8260D 0.704 1.00 20.00 0 91.7 µg/L SW8260D 0.436 1.00 20.00 0 96.2 µg/L SW8260D 0.285 1.00 20.00 0 90.0 µg/L SW8260D 0.575 1.00 60.00 0 91.5 µg/L SW8260D 50.00 100 µg/L SW8260D 50.00 94.0 µg/L SW8260D 50.00 97.l µg/L SW8260D 50.00 94.9 Limits 74 -236 70 -350 80 -127 66 -143 85 -124 30 -149 65 -154 55 -128 59 -135 69 -129 66 -124 80 -136 85 -121 78 -132 81 -123 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual Report Date: 4/10/2020 Page 23 of 26 analyses applicable to the CWA. SDWA, and RCRA ar-c perfonned in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of tt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2003627 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: MB VOC-1 032720B Date Analyzed: Test Code: 82600-W-DENlOO 2-Butanone <20.0 Acetone <20.0 Benzene < 1.00 Carbon tetrachloride < 1.00 Chloroform < 1.00 Chloromethane < 1.00 Methylene chloride < 1.00 Naphthalene < 1.00 Tetrah ydrofuran < 1.00 Toluene < 1.00 Xylenes, Total < 1.00 Surr: l ,2-Dichloroethane-d4 52.2 Surr: 4-Bromofluorobenzene 50.6 Surr: Dibromofluoromethane 48.7 Surr: Toluene-d8 49.3 Units 3440 South 700 West Salt Lake City, UT 841 I 9 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Method MDL Limit Tanner Holliday MSVOA MBLK Spike Ref. Amount %REC 03/27/2020 1319h µg/L SW8260D 1.22 20.0 µg/L SW8260D 2.76 20.0 µg/L SW8260D 0.147 1.00 µg/L SW8260D 0.859 1.00 µg/L SW8260D 0.166 1.00 µg/L SW8260D 0.802 1.00 µg/L SW8260D 0.381 1.00 µg/L SW8260D 0.704 1.00 µg/L SW8260D 0.436 1.00 µg/L SW8260D 0.285 1.00 µg/L SW8260D 0.575 1.00 µg/L SW8260D 50.00 104 µg/L SW8260D 50.00 101 µg/L SW8260D 50.00 97.4 µg/L SW8260D 50.00 98.6 Limits 80 -136 85 -121 78 -132 81 -123 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPO Limit Qual Report Date: 4/10/2020 Page 24 of 26 analyses applicable to the CWA. SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling infom1ation is located on the attached COC Confidential Business Information: TI1is report is provided for the exclusive use of the addressee. Privileges of subsequent use oftt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement., promotion or saJe of any product or process, or in connection with the re-publication of this report for any pwpose other than for the addressee wi11 be granted only on contact. This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2003627 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: 2003627-00IAMS Date Analyzed: Test Code: 8260D-W-DEN100 2-Butanone 21.3 Acetone 18.4 Benzene 18.6 Carbon tetrachloride 18.7 Chloroform 19.2 Chloromethane 10.2 Methylene chloride 19.1 Naphthalene 17.2 Tetrahydrofuran 18.7 Toluene 17.9 Xylenes, Total 53.9 Surr: l ,2-Dichloroethane-d4 51.0 Surr: 4-Bromofluorobenzene 47.9 Surr: Dibromofluoromethane 48.3 Surr: Toluene-d8 48.0 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Method MDL Limit Tanner Holliday MSVOA MS Spike Ref. Amount %REC 03/27/2020 1438h µg/L SW8260D 1.22 20.0 20.00 0 106 µg/L SW8260D 2.76 20.0 20.00 0 92.2 µg/L SW8260D 0.147 1.00 20.00 0 93.2 µg/L SW8260D 0.859 1.00 20.00 0 93.3 µg/L SW8260D 0.166 1.00 20.00 0 96.1 µg/L SW8260D 0.802 1.00 20.00 0 51.2 µg/L SW8260D 0.381 1.00 20.00 0 95.6 µg/L SW8260D 0.704 1.00 20.00 0 86.1 µg/L SW8260D 0.436 1.00 20.00 0 93.4 µg/L SW8260D 0.285 1.00 20.00 0 89.4 µg/L SW8260D 0.575 1.00 60.00 0 89.9 µg/L SW8260D 50.00 102 µg/L SW8260D 50.00 95.9 µg/L SW8260D 50.00 96.6 µg/L SW8260D 50.00 96.1 Limits 74 -236 70 -350 80 -127 66 -143 85 -124 30 -149 65 -154 55 -128 59 -135 69 -129 66 -124 80 -136 85 -121 78 -132 81 -123 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPO Limit Qual Report Date: 4/10/2020 Page 25 of26 analyses applicable to the CW A. SDW A, and RCRA are perfonned in accordance to NELAC protocols. Pertinent sampling infonnation is located on the attached COC. Confidential Business lnfonnation: TI1is report is provided for the exclusive use of the addressee. Privileges of subsequent use oftJ- ne of this company or any member of its staff~ or reproduction of this report in connection with the advertisement,. promotion or sa1e of any product or process~ or in connection with the re-publication of this report for any purpose other than for the addressee wi11 be granted only on contact. This 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com Jose Rocha QA Officer American West _QC SUMMARY REPORT ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2003627 Dept: MSVOA Project: Annual Seeps & Springs 2020 QC Type: MSD -- Reporting Amount Spiked Spike Ref. RPDRef. RPO Analyte Result Units Method MDL Limit Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 2003627-00IAMSD Date Analyzed: 03/27/2020 1458h Test Code: 8260D-W-DENIOO 2-Butanone 25.0 µg/L SW8260D 1.22 20.0 20.00 0 125 74 -236 21.3 16.2 35 Acetone 21.2 µg/L SW8260D 2.76 20.0 20.00 0 106 70 -350 18.4 13.9 35 Benzene 21.3 µg/L SW8260D 0.147 1.00 20.00 0 106 80 -127 18.6 13.4 35 Carbon tetrachloride 21.6 µg/L SW8260D 0.859 1.00 20.00 0 108 66 -143 18.7 14.6 35 Chloroform 21.4 µg/L SW8260D 0.166 1.00 20.00 0 107 85 -124 19.2 10.5 35 Chloromethane 11.3 µg/L SW8260D 0.802 1.00 20.00 0 56.6 30 -149 10.2 IO.I 35 Methylene chloride 22.1 µg/L SW8260D 0.381 1.00 20.00 0 110 65 -154 19.1 14.3 35 Naphthalene 20.2 µg/L SW8260D 0.704 1.00 20.00 0 101 55 -128 17.2 15.7 35 Tetrahydrofuran 22.3 µg/L SW8260D 0.436 1.00 20.00 0 112 59 -135 18.7 17.7 35 Toluene 20.5 µg/L SW8260D 0.285 1.00 20.00 0 102 69 -129 17.9 13.5 35 Xylenes, Total 61.4 µg/L SW8260D 0.575 1.00 60.00 0 102 66-124 53.9 13.0 35 Surr: l,2-Dichloroethane-d4 51.9 µg/L SW8260D 50.00 104 80 -136 Surr: 4-Bromofluorobenzene 48.8 µg/L SW8260D 50.00 97.7 85 -121 Surr: Dibromofluoromethane 49.5 µg/L SW8260D 50.00 99.0 78 -132 Surr: Toluene-d8 48.5 µg/L SW8260D 50.00 96.9 81 -123 Report Date: 4/10/2020 Page 26 of26 analyses apphcable to the CW A. SOW A. and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee. Privileges of subsequent~ of tt ne of this company or any member of its staff~ or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact, This American West Analytical Laboratories Rpt Emailed: UL Denison WORK ORDER Summary WorkOrder: 2003627 Due Date: 4/10/2020 Page I of I Client: Client ID: Project: Comments: Sample ID 2003627-00IA 2003627-001 B 2003627-00IC 2003627-00ID 2003627-00IE 2003627-002A Printed: 03/27 /20 12:45 Energy Fuels Resources, Inc. ENE300 Contact: Tanner Holliday Annual Seeps & Springs 2020 QC Level: III WO Type: Project QC 3 (no chromatograms). EDD-Denison. CC KWeinel@energyfuels.com; Samples were field filtered for metals; ~ Client Sample ID Collected Date Westwater Spring 3/25/2020 1300h Received Date Test Code Matrix Sel Storage 3/27/2020 1100h 82600-W-DENIOO Aqueous [;,J VOCFridge ____ Te~t_G!:_oup: 8260D:_W-DENJOO; _# of. Analytes: l_lj__#_ o/~ur!.~_4__ .. ·- 300.0-W [v'J df -WC _., ·----3 SEL Analyre.s: CL F S04 ALK-W-23208-LL [,jj df-wc -· ·----·-··----·----·--·-____ -·· -·---_ _2SELAnalytes:ALKBALKC ---------·· .. --. - ---·-----4 ----------. ____ ,,_ __ .. ·----- ---·--------- TDS-W-2540C ~] df-tds ______ I SELAnalyie.s: TDS NHJ-W-350.1 _____ I Sf}L An<!!J.tes:!jH3N_ NH3-W-PR ·-------------·---. N02/N03-W-353.2 ___ _ _ I 8_EL Anatytes: NC?_3N02!:f __ _ 200.7-DIS -------·-__ 4.SEL Analyt~: CA ~G_§._N_'.4 _______ _ 200.7-DIS-PR ------------------200.8-DIS J;;,J df -no2/no3 & nh3 ~~-no:f_n~nh3 r;,1 df -no2/no3 & nh3 J,tJ df-met ~ J,tj df-met df-met 18 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUVZN 200.8-DIS-PR ----·--·-·--. ----··---·----- HG-DW-DIS-245.1 ··-·-___ J,;,L [~j df-met df-met ---------· .. --. _ -------·----------__ .. ____ . ______ ISEL Analyte.s:HG _______ _ ___ ----· ___ -----·---·--•·---------· ---·-·-· -· .. HG-OW-DIS-PR -·-··-.. _______________ ['ll] df-met IONBALANCE J..tJ df-met 5 S§J:.1..'!!!/;:(es: 1!._A_L_ANCE Anions_ Cations TDS-Jla'EFI!!!. '!!l_S:..Cal~ Trip Blank 3/25/2020 1300h 3/27/2020 1100h 8260D-W-DEN100 Aqueous [;,] VOCFridge 7:est_~'21Uf:..f!J_60D-W-Df!!'!_IO~;_#~f A_n_qq;tes: 111# of ~u:;: 4 LABORATORY CHECK: %M [] RT [l CN O TAT[] QC [J LUO[] HOK ___ HOK __ _ HOK___ COC Emailed~---- 3 3 5 8 ' 10 ) I ! Address: Contact: Phone#: Email: Project Name: Project#: PO#: Sampler Name: Westwater Spring Trip Blank American West Analytical Laboratories 463 W. 3600 S. Salt Lake City, UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 6425 S. Hwy. 191 Blanding, UT 84511 Tanner Holliday (4351678-2221 Cell#: gpalmel@eneqyfaels.com; KWeiDel@energyfuels.com; tholllda!J!l!ne!lllfuels.com Annual Seeps & Springs 2020 Tanner Holliday Date Samele ID: Samoled I 3/25/2020 3/25/2020 Date: Rel!llqlJlslled by.~. $lnl\3!Urn '-,I ~ r> A ~././£_/ = C,/ mme: "ml Name: Tanner Hol~-· 110C Retnqulshed by. Dale: ~ ........ _ Time: """'Narno: Roltlquisned by: Date: """natU'e Tim&: Ptlnl Name: Relmqulshed by. ,.,,,,_ Dale: Time: Pl1n1Name: Time Sampled 1300 1300 Rec,,l\oedby. Si<lnahlre Print N""'e: Received by: Si<lnanre Print Name: Received by: lslQnature Print Name: Received by: !~nature Print Name: I -........ CHAIN OF CUSTQDY All analysis will be conducted using NELAP accredited met:,ods and all data will be reported using AWAL's standard analyte lls!S and reporting limits (POL) unless specifically requested otherwise on tt,is Chain of Custody and/or attached documentaUon. QC Level: I Tum Around Time: Unless other arrangements have been made, signed repor1s wil be emailed by 5;00 pm on 3 Standard Ille day they an, duo. X Include EDD: 0 LOCUS UPLOAD ;:;; as u EXCEL bD bD X Reid FIitered For: ..... :i:: ;:;; Diasolved Metals .... cl' lti ;:;; :,,:· 'I" C'I .0 as· ~ 0.. z For Compliance With: c:i Cl) ~-0 NELAP 0 i:t. 0 RCRA o' C'I >" c:i ~ ::i 0 CWA 0 c:i u ::i 0 SDWA ..... "' 0 0 ELAP/A2LA .... w 0 c:i ... t'!. C) ci' 0 0 NLLAP IJ) rn ~ 0 ~ .. ,: 0 Non-Compliance "' 0 iii C) ¢ ~ ... IJ) t'!. ... 0 Other: 0 :t. GI 'd. i D' II! ~ c:, D' '5 :El u i 0 " f 0 ""' 0 \0 i:: (I) 0 i ;,:; .!:! 'II Cl) Cl) C'I ]j "' 0 IJ) GI co rn ~ i:: ::;; Ii!; :t. t'!. Ill .e Known Hazards 0 ~ -cf -0 "' i Ill • u a. Ci I Ill '5 • < 0 & 0 E 0 &: ~ • R g .. 2: {,) iS 0 Samole Comments .. Cl) ... 7 w X X X X X X X X X X 3 w X J..bo3LRd:7 AWAL Lab Sample Set# Page 1 of 1 Due Date: 4 \tb \1t> Laboratory Use Only Samples Were: ~ :~•\>'' 3 Temperature ;).. Q •c 4 Recelvedv (Im property ' y 5~N ~;~ c;ngTI-N Ir.cc Tape Was: 1 Present z::;, Pacl<.lge Y N NA 2 Unbroken on OUter!"~ Y N NA 3 PresentonB Y N NA 4 Unbroken on Sample A Y N NA -Discrepancies Between Sample y N abels and COC R~ .:::..,,r~-~< ./, Dal',~ ,I 3-0 Special Instructions: .J~ n4"1("".{(. 1-, +" ., .. e, \\.00 Sample containers for metals were field filtered. See the Date: Analytical Scope of Work for Reporting Limits and voe analyte rnme: list. Date: ·nme: Date: nme: Analysis Ammonia COD Cyanide Metals N02/N03 O&G Phenols Sulfide TKN TP04 CrVI+ Procedure: Frequency: Preservation Check Sheet s am le SetE Pl Preservative \ pH<2H2S04 "~ oH<2H2S04 oH>l2NaOH pH<2HN03 " "'"' oH<2H2S04 '{ t<:. pH<2HCL oH<2H2S04 pH>9NaOH, Zn Acetate pH<2 H2S04 oH<2 H2S04 pH>9 (NH4)2S04 Pour a small amount of sample in the sample lid Pour sample from lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid d pH . 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + • # • The sample required additional preservative upon receipt. The sample was received unpreserved. The sample was received unpreserved and therefore preserved upon receipt. The sample pH was unadjustable to a pH < 2 due to the sample matrix. The sample pH was unadjustable to a pH> __ due to the sample matrix interference . Lab Set ID: pH Lot#: ~oc3ud-1 u,li ~ le;t ~ I I Laboratories LLc a member of The GEL Group INC PO Bo,30712 Cha~eston.SC29417 2040 Sa•1age Road Cha~eston. SC 29407 P 843 556.8171 F 8437661178 April 14, 2020 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: Analytical for Annual Seeps and Spring 2020 Work Order: 508151 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on March 31, 2020. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies of GEL' s accreditations and certifications can be found on our website at www .gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DW16138 Enclosures Sincerely, ~ j,tJ Samuel Hogan for Julie Robinson Project Manager ilH UHlll 1111111111111111 U II gel.com Page 2 of 13 SDG: 508151 Energy Fuels Resources (USA), Inc. Analytical for SDG: 508151 April 14, 2020 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 508151 Sam pie receipt: The sample arrived at GEL Laboratories LLC, Charleston, South Carolina on March 31, 2020 for analysis. The sample was delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following sample: Laboratory ID Client ID 508151001 Westwater Spring Case Narrative: Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Page 3 of 13 SDG: 508151 ~~ Samuel Hogan for Julie Robinson Project Manager ~-/~~~ s:;;i-,;NERGYFUELS RESOURCES Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: GEL Laboratories, LLC Contact: Tanner Holliday -2-04_0__,...S-av_a_g_e_R_o_a_d________ Ph : 435 678 2221 Charleston, SC 29407 tholliday@enerqyfuels.com (843) 556 8171 Chain of Custody/Sampling Analysis Request p . t roJec s amp1ers N ame s amp1ers s· t 1gna ure Annual Seeps & Springs L-· )r,\ A 11 iJ ...-)/~/-,/ 2020 Tanner Holliday / Time Sample ID Date Collected Collected Laboratory Analysis Requested Westwater Spring 3/25/2020 1300 Gross Alpha Comments: Please send report to Kathv Weinel at kweinel@enerovtuels.com Relinquished By:(Signature) Page 4 of 13 SDG: 508151 Date/Time Received By:(Signature) 3/26/2020 1100 ~ i l ,:n'.~a:o:;e:). ;; r& SI ... MPfL.~ t~!ECE.tPT _&_l_l_£_v_r_E_~_;_-t_·~-R_M_1~~-~-"--':....!=-_ ....;'l)__;(.....;.;;;....:...._;......:.=:....·-:..;.~-~i_l'._i~'.· ~'.fcn,:.--......,.--..l ... D. .... W.....,.W.~:i;____-_ --. _·_· -·~}.l~C?0;;,?::~~-. 1 · ·' ... . . .: ~ .... ::·~ • :'._":' _I f, I , i"': ' 1 • I 1'! ·,;·•1; R~cciv ~ti lly: _ P.al•! ~~ 3' §_lp.i_.....:_...:..;.:.....;....:......:.. __ -'·;_,_·_--....:.-"--..:.......;;c.....: __ =·'-:-', -· :...;.:._' ;.:;· '.;..........;-=---1 -* • .. -• Cir.::k~..ibk: f Fcdtx Express l'cdEx Ground & l'icld Services Courier Other 17-ttt'f Ylf.YtJ;·f%.z <i5tf7 Cn~rlcr nr,:: Tniclling Number ! , ., 1----------------------1-------·--··· _._ ________ .:.....;:....._ ...... _.....::..... __ .....:;.::. __ ..;.;..__;:,.:_...:.._~::,:c=.....:::........::---1 S11s11ec1cd Mn>.ard. lnfo,·nrn1ion ;. I_ • If Net Cn1111s > •. ! OOcp,n on-samples not nrnrkcd "rndionc1ive''.'cci1i1act ilii: Radintio11 Safety Group fclr h,rihcr i11vc':;li!falion. 1-----------------+--,-,--+----·-·---------------·---·--....:..-----=----'-· ... i.. ---. ,\JShi111ed as a DOT Hnz~rdous'! B) Did the clicnl desib~1.nlc the samples arc 10 be roccivc<l as r.adivacti ve'' C) Did the RSO classify the samples as '"' rndioncrivc'f D) Did the client designate samples nre hn'1,1rdous'! EJ Diu ihc RSO ide111/fv ossiblc hn1.nrds'/ S11m11I" Ucccipt Crllcrln Shipping containers received i111acl and sealed? 2 Chain or custody documents included with shipm.c_•1_ll_? _________ -+· 3 Samples requiring cold preservation within (0 :: 6 deg. C)?• ' Dnil); check performed and passed on IR 4 t~mpernture gun? 5 S0111plc containers intact a,;d scaled'! Sump cs rcquirfng chemical pri:~cn~ntion ~ 111 ,,roper pH? Do uny snmples require Volniilc Analysis? E S,11nplcs recciwd within holding lime? 9 Sample ID's on COC match ID's on boltles'? 10 Dale & lime on COC match date &,iime oi1 llonles~ 11 N uml>.:r of conrainers received nm1ch number indicated on COC'' 12 A're smnpl.: containers identifiable as · C:E r v' l•t!·• 13 COC form is properly signed in n:linquishcd/roccivcd scc1ions'! Commcil\s ( Use Co11ti111m1io11 l'onn if needed): Hn,.,rd Class Shi11ptd: UN#: If UN2910, I~ the Radioncti1·0 Shi11111ent Sun·cy Cnmpl ant? ,Yes_ .No_ COC notation or rndio3crivc :slickers on contafoc.rs c'qiml clic'nr dcs t1nntio11. Masi,mun Net Counts Observed• (Obsen•ed Counts• /\rcn llackgro1111d Counls): ~cr~l / mRll·f r Clr.ssifkd ns: a.ml I R:ui 2 Rntl J . 1 • COC' notnt/on nr ha111rd ln\,eis 011 cnmainers cqunt clic0n1 dl!Signntioi'r. l'lammablc foreign Soil RCR;\ Asbestos llcrylli11111 01her: Commenrs/Quali,liers (ncr1uirct1 for Non-Conforn.1ing Items): rirclc ,lpplicablc: Lcaki11y contoiner. Other (describe) 'Chclc Applicublo:: Client co11tnctcd nnd prO\'ideJ C.'OC COC:'e1co1cd """" rocclp1 l'rcservaiimi;\.lctl!od:We, It: Ice Packs· . Dry ice No11c Other: fall tcmpcrn1urcs arc recorded in Celsius 'l'cm11crnh1re Dc,ice Serfn"iil:_.,o.;..J!;l.:"j...;.:::.ld:2.. Secondary Temperature De1·ice Serial Ji (If Applicable): Circ.lt: Ap1;!ic!1hlc:: Sc,,ls hrot.:,m O.inuiscd conuuncr Lt:aking co1uai,1cr Other (dderiUC) S:unptt lD's 3nd Cont;tincrs .-\tTcc1cd· . '~ ·, -~ .. • ~_J ·~ I Do liquid VO,\ \·ials ~1.11nin acid prc,ervatio11?:Ycs_ .'lo...:_ NA,.._(frunknown. select ~ol 1 .-\re liquid VOA vinl.< fre~ ofh•;ads1111ce0 Ye.,_ No __ , NA_ · : Smnplt;! Ill's .1nd co111m11crs affl!cl~d ~· I !O's nnd tcsrs nffoc1c.l: IO's and contniilcr~ ~t'fc~1cd·-:------------------------'--.;._. ---.-. Circhl A11plic,1ble: No dates Oil contniilcrs No limes on c0111ni11c1~ COC 111issi11~ in lo. Otl,cr (describe) ' . ,.1 Crrctc Applic,,blc: No co111aiilcr coun1 Oil COC 01hcr (describe) Circle :\ppl!callk Nfll dinc1uishcd 01he1.'(dcscribc) .. , PM (or PMA) review: Initials .~. _____ Date -· -·· Page J_ ol' -~-GL-CHL-SR-001 Rev 6 Page 5 of 13 SDG: 508151 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 508151 Client SDG: 508151 Annual Seeps and Spring 2020 Project Manager: Project Name: Purchase Order: Package Level: EDD Format: Julie Robinson DNMI00106 Analytical for DW16138 LEVEL3 EIM_DNMI GELID Client Sample ID Client Sample Desc. Collect Date& Time Work Order Due Date: 27-APR-20 Package Due Date: EDD Due Date: QA Due Date: IAQJ!I Date: Receive Time # of Date & Time Zone Cont. 25-APR-20 27-APR-20 27-APR-20 28-APR-20 Lab Matrix Report Date: 14-APR-20 Work Order:508151 Page 1 of 2 Collector: C Prelogin #: 20190486669 Project Workdef ID: 1329132 SDG Status: Closed Logged by: Fax Days to Due Date Process CofC# Prelog Lab Field Group QC QC 508151001 Westwater Spring 25-MAR-20 13:00 31-MAR-20 10:45 -2 GROUND WATER 19 Client Sample ID -001 Westwater Spring Status Tests/Methods REVW GFPC, Total Alpha Radium, Liquid Product Reference Gross Alpha Fax Date PM Comments Aux Data Product: GFCTORAL Workdef ID: 1461303 In Product Group? No Group Name: Group Reference: Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Samples: 001 Parmname Check: All parmnames scheduled properly CAS# Contingent Tests Parmname Gross Radium Alpha Action Product Name Login Requirements: Requirement Description Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Client RDL or PQL& Unit Reporting Parm Included Included Custom Units Function in Sample? in QC? List? pCi/L REG y y No Samples Include? Comments Receive Codes ...... lf) ...... 00 0 lf) c:, Cl r./) (") '+-< 0 \0 ~ ~ 0.... GEL Laboratories LLC -Login Review Report Peer Review by: ____________ _ Work Order (SDG#), PO# Checked? ____ _ Report Date: 14-APR-20 Work Order: 508151 Page 2 of 2 C of C signed in receiver location? _____ _ ...... V) ...... 00 0 V) 0 0 rJJ. ("<") ...... (+-, 0 t"-- (1) ~ ~ List of current GEL Certifications as of 14 April 2020 State Certification Alaska 17-018 Alaska Drinking Water SC00012 Arkansas 88-0651 CUA 4200904046 California 2940 Colorado SC00012 Connecticut PH-0169 DoD ELAP/ ISOl 7025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-15-00283,P330-15-00253 Georgia SC00012 Georgia SOWA 967 Hawaii SCOOOJ2 Idaho SCOOOJ2 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SOWA 90129 Kentucky Wastewater 90129 Louisiana Drinking Water LA024 Louisiana NELAP 03046 (AI33904) Maine 2019020 Maryland 270 Massachusetts M-SC012 Massachusetts PF AS Approv Letter Michigan 9976 Mississippi SC00012 Nebraska NE-OS-26-13 Nevada scooo 122020-1 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 2019-165 Pennsylvania NELAP 68-00485 Puerto Rico SC00012 S. Carolina Radiochem 10120002 Sanitation Districts of L 9255651 South Carolina Chemistry 10120001 Tennessee TN 02934 TexasNELAP TI04704235-20-16 UtahNELAP SCOOOI22020-32 Vermont VT87156 Virginia NELAP 460202 Washington C780 Page 8 of 13 SDG: 508151 Radiochemistry Technical Case Narrative Energy Fuels Resources SDG #: 508151 Product: GFPC, Total Alpha Radium, Liquid Analytical Method: EPA 903.0 Analytical Procedure: GL-RAD-A-044 REV# 10 Analytical Batch: 1987404 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 508151001 1204540495 1204540496 1204540497 1204540498 1204540499 Client Sam pie Identification Westwater Spring Method Blank (MB) 50815100 I (Westwater Spring) Sample Duplicate (DUP) 50815100l(Westwater Spring) Matrix Spike (MS) 508151001(Westwater Spring) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Preparation Information Aliquot Reduced aliquots were reduced due to limited sample volume. Miscellaneous Information Additional Comments The matrix spike and matrix spike duplicate, 1204540497 (Westwater SpringMS) and 1204540498 (Westwater SpringMSD), aliquots were reduced to conserve sample volume. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 9 of 13 SDG: 508151 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMIOOI Energy Fuels Resources (USA), Inc. Client SDG: 508151 GEL Work Order: 508151 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. ReviewN alidation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: j~ ~ Name: Theresa Austin Date: 16 APR 2020 Title: Group Leader Page 10 of 13 SDG: 508151 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summarr Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Contact: Ms. Kathy Weinel Workorder: 508151 Parm name NOM Rad Gas Flow 3atch 1987404 QC1204540496 508151001 DUP Gross Radium Alpha u 0.559 u Uncertainty +l-0.300 QC1204540499 LCS Gross Radium Alpha 739 Uncertainty QC1204540495 MB Gross Radium Alpha u Uncertainty QC 1204540497 508151001 MS Gross Radium Alpha 4470 u 0.559 Uncertainty +l-0.300 QC 1204540498 508151001 MSD Gross Radium Alpha 4470 u 0.559 Uncertainty +l-0.300 Notes: Counting Uncertainty is calculated at the 68% confidence level (]-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product C Units -0.0904 pCilL +l-0.198 766 pCilL +l-9.24 0.310 pCilL +l-0.261 5060 pCilL +l-56.2 5090 pCi/L +l-55.5 RPO% NIA 0.764 A B BD C D F H K L M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Page 12 of 13 SDG: 508151 Report Date: April 14, 2020 REC% Rane Anlst NIA JXK3 104 (75%-125%) 113 (75%-125%) 114 (0%-20%) Page 1 of Date Time 04113120 13: 1, 04113120 13: 1, 04113120 13: l 1 04113120 13: I• 04113120 13 :1, GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 508151 Parmname NOM Sam ual QG __ U~nc..cit-'-s _--=.cR=PD% REC% Rang~Anlst M Matrix Related Failure NIA RPD or %Recovery limits do not apply. NI ND NJ Q R u UI UJ UL X y I\ h See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of Date Time NI A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. "The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +I-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 13 of 13 SDG: 508151 3440 South 700 West ,alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Tanner Holliday Energy Fuels Resources, Inc. 6425 South Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: Annual Seeps & Springs 2020 Dear Tanner Holliday: Lab Set ID: 2006528 American West Analytical Laboratories received sample( s) on 6/18/2020 for the analyses presented in the following report. American West Analytical Laboratories (AW AL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, Wyoming, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Approved by: J G Digitally signed 058 . by Jose G. Rocha Rocha Date: 2020.07.06 16:35:43 -06'00' Laboratory Director or designee Report Date: 7/6/2020 Page I of38 All analyses applicable to lhe CWA. SDWA, and RCRA are performed in accordance lo NELAC prolocols Per1inent sampling information is localed on lhe allached COC. Confidenlial Business Information: This report is provided for lhe exclusi\·e use or Lhe ~ddressee Pri, ile~es o.f sub,.5eq~ent ~~e of lhe ~~e of lhis.co~pnny or an) ~mber of its stnIT. or reproduclio~ ~f this repo~ in ~on~eclion .. with the a~ver1isemenl, P~?motio.n or sale of ?1!)~ ~rod~cl or P~?cess, ~r in ~onm~c!ion w!lh lh~ r~-publication of Lhis repon SAMPLE SUMMARY Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday AN"lYrtCAL I AflORATORIFS Project: Annual Seeps & Springs 2020 Lab Set ID: 2006528 Date Received: 6/18/2020 llOOh Lab Sample ID Client Sample ID Date Collected Matrix Analysis 3440 South 700 West 2006528-00 I A Westwater Seep 6/16/2020 845h Aqueous VOA by GC/MS Method ;alt Lake City, UT 84119 8260D/5030C 2006528-001 B Westwater Seep 6/16/2020 845h Aqueous Anions, E300.0 2006528-0018 Westwater Seep 6/16/2020 845h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level Phone: (801) 263-8686 2006528-00 l C Westwater Seep 6/16/2020 845h Aqueous Total Dissolved Solids, A2540C Toll Free: (888) 263-8686 2006528-001 D Westwater Seep 6/16/2020 845h Aqueous Nitrite/Nitrate (as N), E353.2 Fax: (801) 263-8687 2006528-001 D Westwater Seep 6/16/2020 845h Aqueous Ammonia, Aqueous !-mail: awal@awal-labs.com 2006528-00 l E Westwater Seep 6/16/2020 845h Aqueous Ion Balance 2006528-00 l E Westwater Seep 6/16/2020 845h Aqueous ICP Metals, Dissolved web: www.awal-labs.com 2006528-00 l E Westwater Seep 6/16/2020 845h Aqueous ICPMS Metals, Dissolved 2006528-001 E Westwater Seep 6/16/2020 845h Aqueous Mercury, Drinking Water Dissolved Kyle F. Gross 2006528-002A Ruin Spring 6/16/2020 1035h Aqueous VOA by GC/MS Method 8260D/5030C Laboratory Director 2006528-0028 Ruin Spring 6/16/2020 1035h Aqueous Anions, E300.0 2006528-0028 Ruin Spring 6/16/2020 1035h Aqueous Alkalinity/ Bicarbonate/ Jose Rocha Carbonate, Low Level QA Officer 2006528-002C Ruin Spring 6/16/2020 1035h Aqueous Total Dissolved Solids, A2540C 2006528-002D Ruin Spring 6/16/2020 1035h Aqueous Nitrite/Nitrate (as N), E353.2 2006528-002D Ruin Spring 6/16/2020 1035h Aqueous Ammonia, Aqueous 2006528-002E Ruin Spring 6/16/2020 1035h Aqueous Ion Balance 2006528-002E Ruin Spring 6/16/2020 1035h Aqueous ICP Metals, Dissolved 2006528-002E Ruin Spring 6/16/2020 1035h Aqueous ICPMS Metals, Dissolved 2006528-002E Ruin Spring 6/16/2020 1035h Aqueous Mercury, Drinking Water Dissolved 2006528-003A Cottonwood Spring 6/16/2020 945h Aqueous VOA by GC/MS Method 8260D/5030C 2006528-0038 Cottonwood Spring 6/16/2020 945h Aqueous Anions, E300.0 2006528-0038 Cottonwood Spring 6/16/2020 945h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level 2006528-003C Cottonwood Spring 6/16/2020 945h Aqueous Total Dissolved Solids, A2540C 2006528-003D Cottonwood Spring 6/16/2020 945h Aqueous Ammonia, Aqueous 2006528-003D Cottonwood Spring 6/16/2020 945h Aqueous Nitrite/Nitrate (as N), E353.2 2006528-003E Cottonwood Spring 6/16/2020 945h Aqueous Ion Balance 2006528-003E Cottonwood Spring 6/16/2020 945h Aqueous ICP Metals, Dissolved 2006528-003E Cottonwood Spring 6/16/2020 945h Aqueous ICPMS Metals, Dissolved Report Date: 7/6/2020 Page 2 of38 All analyses .ipplicable to lhe CWA. SOWA, and RCRA are performed in accordance to NE LAC protocols, Peninenl sampling infonnalion is located on lhe attached COC Confidential Business lnformalion: This report is pro,•ided for the exclush e use of \he ~ddressee Pri, ile~es o.f sub~seq~cnt ~~e of Lhe ~~e of this .con:ipany or nny ~mber of ils Slaff, or reproductio~ ~r lhis repo~ in ~o~eclion~ with Lhe a~~ertise~nl, P~?motio.n or sale or ~y ~rod~ct or P~?Cess, ~r in ~onn:_c!ion ,, !th Lh? r~-publicaLion of Lhis report Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps & Springs 2020 Lab Set ID: 2006528 ANA i VT ICAL I AFlORATOR1rs Date Received: 6/18/2020 1100h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 2006528-003E Cottonwood Spring 6/16/2020 945h Aqueous Mercury, Drinking Water 3440 South 700 West 2006528-004A Entrance Seep 6/16/2020 Dissolved 1105h Aqueous VOA by GC/MS Method ;alt Lake City, UT 84119 8260D/5030C 2006528-0048 Entrance Seep 6/16/2020 1105h Aqueous Anions, E300.0 2006528-004B Entrance Seep 6/16/2020 1105h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level Phone: (801) 263-8686 2006528-004C Entrance Seep 6/16/2020 1105h Aqueous Total Dissolved Solids, A2540C Toll Free: (888) 263-8686 2006528-004D Entrance Seep 6/16/2020 1105h Aqueous Nitrite/Nitrate (as N), E353.2 Fax: (801) 263-8687 2006528-004D Entrance Seep 6/16/2020 1105h Aqueous Ammonia, Aqueous !-mail: awal@awal-labs.com 2006528-004E Entrance Seep 6/16/2020 1105h Aqueous ICP Metals, Dissolved 2006528-004E Entrance Seep 6/16/2020 1105h Aqueous ICPMS Metals, Dissolved web: www.awal-labs.com 2006528-004E Entrance Seep 6/16/2020 1105h Aqueous Ion Balance 2006528-004E Entrance Seep 6/16/2020 1105h Aqueous Mercury, Drinking Water Dissolved 2006528-005A Back Spring 6/16/2020 945h Aqueous VOA by GC/MS Method Kyle F. Gross 8260D/5030C Laboratory Director 2006528-0058 Back Spring 6/16/2020 945h Aqueous Anions, E300.0 2006528-005B Back Spring 6/16/2020 945h Aqueous Alkalinity/ Bicarbonate/ Jose Rocha Carbonate, Low Level QA Officer 2006528-005C Back Spring 6/16/2020 945h Aqueous Total Dissolved Solids, A2540C 2006528-005D Back Spring 6/16/2020 945h Aqueous Nitrite/Nitrate (as N), E353.2 2006528-005D Back Spring 6/16/2020 945h Aqueous Ammonia, Aqueous 2006528-005E Back Spring 6/16/2020 945h Aqueous Ion Balance 2006528-005E Back Spring 6/16/2020 945h Aqueous ICP Metals, Dissolved 2006528-005E Back Spring 6/16/2020 945h Aqueous ICPMS Metals, Dissolved 2006528-005E Back Spring 6/16/2020 945h Aqueous Mercury, Drinking Water Dissolved 2006528-006A Trip Blank 6/16/2020 845h Aqueous VOA by GC/MS Method 8260D/5030C Report Date: 7/6/2020 Page 3 of38 All anal~ses applicable lo lhe CWA. SDWA, and RCRA are performed in accordance to NELAC prolocols. Pertinent sampling informalion is located on the allached COC Confidential Business lnformalion: This report is provided for the e'.';Clusi\·e use of [he ~ddressee Pririle~es orsub.seq~en\ ~;ie of the n ... ~e of this .co~pany or an~· ~mber of ils slaff, or reproductio~ ~r1his repo~ in .co~eclion~ with the a~~ertisement, P~?motio;n or sale of~~ ~rodl~I or P~?cess, ~r in ~onn:_c!ion w~lh lh~ r~-publication or this report 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-0-C Discrepancies: Annual Seeps & Springs 2020 2006528 6/18/2020 6/16/2020 Intact None Holding Time and Preservation Requirements: The analysis and preparation of all samples were performed within the method holding times. All samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike / Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exceptions: Sample ID Analyte QC Explanation 2006528-00 IE Calcium MS/MSD High analyte concentration 2006528-001 E Sodium MS/MSD High analyte concentration 2006528-002D Ammonia MS/MSD Sarni ematrix interference Duplicate (DUP): The parameters that required a duplicate analysis had RPDs within the control limits. Corrective Action: None required. Report Date: 7/6/2020 Page 4 of38 All analyses applicable lo the CWA, SOWA. and RCRA are perfom1ed in accordance to NELAC prolocols, Pertinent sampling information is located on the anached COC Confidenti.il Business fnformalion: This report is pro,•ided for the exclusiYe use oflhe ~ddressee Pri, ile~es o_f sub~seq~nl ~~e of lhe ~~e of this .con:ipany or nny ~mber of its staff, or reproductio~ ~~ this repo~ in ~~ecLion~ with the ~vertisement, P~?motio.n or sale of ?-1!Y. ~rod~ct or p~~cess. ~r in ~11ni;c~ion "~lh lh~ ri;-publication of this report 3440 South 700 West ,alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-0-C Discrepancies: Method: Annual Seeps & Springs 2020 2006528 6/18/2020 6/16/2020 Intact None SW-846 8260D/5030C Analysis: Volatile Organic Compounds General Set Comments: One or more target analytes were observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike / Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 7/6/2020 Page 5 of38 All anaJyses applicable LO the CWA. SDWA, and RCRA are perfom1ed in accordance lo NELAC protocols Pertinenl sampling informotion is located on Lhe altached COC Conlidenliol Business Information: This report is provided for lhe exclusi,e use of the ~ddressee Pri\·ile~es o[su~eq~nt ~e of the ?_~e of Lhis .co~pany or M)' '!:mber of its sta1T, or reproduclio~ ~fthis repo~ in ~on~eclion~ with the ~~ertise~ent, P~?moli°:'1 or sale of ~Y. ~rod~ct or p~ocess, ~r in ~nn~~ion w~Lh th? r:-p~blicalion of lhis report 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West QCSUMM_A.RY REPORT ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2006528 Dept: ME Project: Annual Seeps & Springs 2020 QC Type: LCS Reporting Amount Spiked Spike Ref. RPDRef. RPD Aoalyte Result Units Method MDL Limit Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: LCS-70574 Date Analyzed: 07/01/2020 1849h Test Code: 200.7-DIS Date Prepared: 06/19/2020 1313h Calcium 9.94 mg/L E200.7 0.211 1.00 10.00 0 99.4 85 -115 Magnesium 10.0 mg/L E200.7 0.0654 1.00 10.00 0 100 85 -115 Potassium 10.4 mg/L E200.7 0.246 1.00 10.00 0 104 85 -115 Sodium 10.5 mg/L E200,7 0.123 1.00 10.00 0 105 85 -115 Lab Sample ID: LCS-70574 Date Analyzed: 07/03/2020 1155h Test Code: 200.7-DIS Date Prepared: 06/19/2020 1313h Vanadium 0.212 mg/L E200.7 0.00252 0.00500 0.2000 0 106 85 -115 Lab Sample ID: LCS-70576 Date Analyzed: 06/22/2020 1128h Test Code: 200.8-DIS Date Prepared: 06/19/2020 1313h Manganese 0.191 mg/L E200 8 0.000766 0.00200 0.2000 0 95,6 85 -115 Lab Sample ID: LCS-70576 Date Analyzed: 07/01/2020 1311 h Test Code: 200.8-DIS Date Prepared: 06/19/2020 1313h Arsenic 0.188 mg/L E200.8 0.000298 0.00200 0.2000 0 93.9 85 -115 Beryllium 0.206 mg/L E200.8 0.000198 0.00200 0.2000 0 103 85 -115 Cadmium 0.189 mg/L E200.8 0.0000742 0.000500 0.2000 0 94.6 85 -115 Chromium 0.197 mg/L E200.8 0.00191 0.00200 0.2000 0 98.3 85 -115 Cobalt 0.199 mg/L E200,8 0.000300 0.00400 0.2000 0 99.3 85 -115 Copper 0.202 mg/L E200.8 0.00166 0.00200 0.2000 0 101 85 -115 Iron 0.974 mg/L E200.8 0.0328 0.100 1.000 0 97.4 85 -115 Lead 0.198 mg/L E200,8 0.000448 0.00200 0.2000 0 99.0 85 -115 Molybdenum 0.195 mg/L E200,8 0.000652 0.00200 0.2000 0 97.6 85 -115 Nickel 0.198 mg/L E200.8 0.000728 0.00200 0.2000 0 98.9 85 -115 Selenium 0.184 mg/L E200.8 0.000508 0.00200 0.2000 0 92.0 85 -115 Silver 0.190 mg/L E200.8 0.000232 0.00200 0.2000 0 94.9 85 -II 5 Thallium 0.195 mg/L E200 8 0.000390 0.00200 0.2000 0 97.6 85 -115 Report Date: 7/6/2020 Page 22 of38 analyses applicable to the CWA, SOWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee. Privileges of subsequent use oftf ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re•publication of this report for any purpose other than for the addressee will be granted only on contact, This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2006528 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: LCS-70576 Date Anal y,:.ed: Test Code: 200.8-DIS Date Prepared: Tin 0.989 Uranium 0204 inc 0.994 Lab Sample ID: LCS-70662 Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury 0.00339 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QCS1)_MMA&YJIBPO_RT Contact: Dept: Tanner Holliday ME Units Method 07/01/2020 1311h 06/19/2020 1313h mg/L E200,8 mg/L E200.8 mg/L E200.8 -06/25/2020 908h 06/24/2020 1313h mg/L E245.I MDL 0.00115 0.000176 0.00418 0.0000396 Reporting Limit 0.00400 0.00200 0.00600 0.0000900 QC Type: LCS Amount Spiked Spike Ref. 1.000 0.2000 1.000 0.003330 Amount 0 0 0 0 %REC 98.9 102 99.4 102 Limits 85 -115 85 -115 85 -115 85 -115 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Limit Amt %RPO Qua! Report Date: 7/6/2020 Page 23 of38 analyses applicable to the CWA, SOWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of fr ne of th.is company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This A.merican West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2006528 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: MB-70574 Date Analyzed: Test Code: 200.7-DIS Date Prepared: Calcium < 1.00 Magnesium < 1.00 Potassium < 1.00 Sodium < 1.00 Lab Sample ID: MB-70574 Date Analyzed: Test Code: 200.7-DIS Date Prepared: Vanadium < 0.00500 Lab Sample ID: MB-70576 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Manganese < 0.00200 -Lab Sample ID: MB-FILTER-70557 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Manganese < 0.00200 Lab Sample ID: MB-70576 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Arsenic < 0.000200 Beryllium < 0.000200 Cadmium < 0.0000500 Chromium < 0.000200 Cobalt < 0.000400 Copper < 0.000200 Iron < 0.0100 Lead < 0.000200 Molybdenum < 0.000200 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARYREPORT Contact: Dept: QC Type: Reporting Amount Spiked Units Method MDL Limit 07/01/2020 1846h 06/19/2020 1313h mg/L E200.7 0.211 1.00 mg/L E200.7 0.0654 1.00 mg/L E200.7 0.246 1.00 mg/L E200.7 0.123 1.00 -07/03/2020 1152h 06/19/2020 1313h mg/L E200.7 0.00252 0.00500 06/22/2020 1124h 06/19/2020 13 I Jh n:ig;IL E200.8 0.000766 0.00200 -06/22/2020 1152h 06/19/2020 1313h mg/L E200.8 0.000766 0.00200 -07/01/2020 1308h 06/19/2020 1313h mg/L E200.8 0.0000298 0.000200 mg/L E200.8 0.0000198 0.000200 mg/L E200.8 0.00000742 0.0000500 mg/L E200.8 0.000191 0.000200 mg/L E200.8 0.0000300 0.000400 mg/L E200.8 0.000166 0.000200 mg/L E200.8 0.00328 0.0100 mg/L E200.8 0.0000448 0.000200 mg/L E200.8 0.0000652 0.000200 Tanner Holliday ME MBLK Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 7/6/2020 Page 24 of38 analyses applicable to the CWA, SOWA, and RCRA are performed in accordance to NELAC protocols, Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use oftl- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This Am,erican West ANALYTICAL LABORATOAtES Client: Energy Fuels Resources, Inc. Lab Set ID: 2006528 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: MB-70576 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Nickel < 0.000200 Selenium < 0.000200 Silver < 0.000200 Thallium < 0.000200 Tin < 0.000400 Uranium < 0.000200 Zinc < 0.000600 Lab Sample ID: MB-70662 Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury < 0.0000900 Lab Sample ID: MB-FILTER-70655 Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury < 0.0000900 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Units Method MDL Limit 07/01/2020 1308h 06/19/2020 1313h mg/L E200.8 0.0000728 0.000200 mg/L E200 8 0.0000508 0.000200 mg/L E200.8 0.0000232 0.000200 mg/L E200.8 0.0000390 0.000200 mg/L E200 8 0.000115 0.000400 mg/L E200.8 0.0000176 0.000200 mg/L E200.8 0.000418 0.000600 -06/25/2020 906h 06/24/2020 1313 h mg/L E245.l 0.0000396 0.0000900 06/25/2020 936h 06/24/2020 1313h mg/L E245 .l 0.0000396 0.0000900 Tanner Holliday ME MBLK Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPO Limit Qual Report Date: 7/6/2020 Page 25 of38 analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to NE LAC protocols. Pertinent sampling infonnation is located on the attached COC Confidential Business lnfonnation: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee wi11 be granted only on contact Thls 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West QC SUMMARY REPORT ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2006528 Dept: ME Project: Annual Seeps & Springs 2020 QC Type: MS Reporting Amount Spiked Spike Ref. RPO Ref. RPO Analyte Result Units Method MDL Limit Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 2006528-00 lEMS Date Analyzed: 07/01/2020 1859h Test Code: 200.7-DIS Date Prepared: 06/19/2020 1313h Calcium 218 mg/L E200.7 2.11 10.0 10.00 204 146 70 -130 Magnesium 65.6 mg/L E200,7 0.654 10.0 10.00 54.6 109 70 -130 Sodium 262 mg/L E200.7 1.23 10.0 10.00 245 166 70 -130 Lab Sample ID: 2006528-00IEMS Date Analyzed: 07/03/2020 1200h Tes1 Code: 200.7-DIS Date Prepared: 06/19/2020 1313h Potassium 16.7 mg/L E200.7 0.246 LOO 10.00 5.28 114 70 -130 Vanadium 0.230 mg/L E200,7 0.00252 0.00500 0.2000 0 115 70 -130 Lab Sample ID: 2006528-00IEMS Date Analyzed: 06/22/2020 1145h Test Code: 200.8-DIS Date Prepared: 06/19/2020 1313h Manganese 0.231 mg/L E200.8 0.000766 0.00200 0.2000 0.0354 97.7 75 -125 Lab Sample ID: 2006528-00IEMS Date Analyzed: 07/01/2020 1317h Test Code: 200.8-DIS Date Prepared: 06/19/2020 1313h Arsenic 0.206 mg/L E200,8 0.000298 0.00200 0.2000 0.00157 102 75 -125 Beryllium 0.220 mg/L E200,8 0.000198 0.00200 0.2000 0 110 75 -125 Cadmium 0.199 mg/L E200.8 0.0000742 0.000500 0.2000 0 99.4 75 -125 Chromium 0.206 mg/L E200.8 0.00191 0.00200 0.2000 0 103 75 -125 Cobalt 0.207 mg/L E200.8 0.000300 0.00400 0.2000 0.00046 103 75 -125 Copper 0.211 mg/L E200.8 0.00166 0.00200 0.2000 0 105 75 -125 Iron 1.04 mg/L E200.8 0.0328 0.100 1.000 0 104 75 -125 Lead 0.209 mg/L E200,8 0.000448 0.00200 0.2000 0 104 75 -125 Molybdenum 0.218 mg/L E200.8 0.000652 0.00200 0.2000 0.00933 105 75 -125 Nickel 0.207 mg/L E200.8 0.000728 0.00200 0.2000 0.000968 103 75 -125 Selenium 0.197 mg/L E200.8 0.000508 0.00200 0.2000 0.00121 97.8 75 -125 Silver 0.196 mg/L E200.8 0.000232 0.00200 0.2000 0 98.1 75 -125 Thallium 0.206 mg/L E200.8 0.000390 0.00200 0.2000 0 103 75 -125 Report Date: 7/6/2020 Page 26 of38 analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee, Privileges of subsequent use oftt ne of trus company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee wi11 be granted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2006528 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: 2006528-00 I EMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Tin 1.06 Uranium 0.233 Zinc 1.05 Lab Sample ID: 2006528-002EMS Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury 0.00348 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMA.RY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Units Method MDL Limit 07/01/2020 131 7h 06/19/2020 1313h mg/L E200.8 0.00115 0.00400 1.000 mg/L E200.8 0.000176 0.00200 0.2000 mg/L E200.8 0.00418 0.00600 1.000 -06/25/2020 918h 06/24/2020 1313h mg/L E245.I 0.0000396 0.0000900 0.003330 Tanner Holliday ME MS Spike Ref. Amount %REC 0 106 0.0129 110 0 105 0 105 2 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD. Limits 75 -125 75 -125 75 -125 85 -I I 5 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit Qual Report Date: 7/6/2020 Page 27 of38 analyses applicable to the CWA, SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use oftl- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re·publication of this report for any purpose other than for the addressee will be granted only on contact This 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West QC SUMMA.RY REPORT ANALVTJCAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2006528 Dept: ME Project: Annual Seeps & Springs 2020 QC Type: MSD Reporting Amount Spiked Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 2006528-001 EMSD Date Analyzed: 07 /0 I /2020 1902h Test Code: 200.7-DIS Date Prepared: 06/19/2020 1313h Calcium 217 mg/L E200,7 2.11 10.0 10.00 204 135 70 -130 218 0.504 20 Magnesium 67.0 mg/L E200.7 0.654 10.0 10.00 54.6 124 70 -130 65 .6 2.13 20 Sodium 262 mg/L E200.7 1.23 10.0 10.00 245 164 70 -130 262 0.0685 20 Lab Sample ID: 2006528-001 EMSD Date Analyzed: 07/03/2020 1203h Test Code: 200.7-DIS Date Prepared: 06/19/2020 1313h Potassium 16.6 mg/L E200,7 0.246 1.00 10.00 5.28 114 70 -130 16.7 0.303 20 Vanadium 0.219 mg/L E200.7 0.00252 0.00500 0.2000 0 109 70 -130 0.23 4.88 20 Lab Sample ID: 2006528-00IEMSD Date Analyzed: 06/22/2020 1148h Test Code: 200.8-DIS Date Prepared: 06/19/2020 1313h Manganese 0.227 mg/L E200.8 0.000766 0.00200 0.2000 0.0354 95.6 75 -125 0.231 1.79 20 Lab Sample ID: 2006528-00IEMSD Date Analyzed: 07/01/2020 1324h Test Code: 200.8-DIS Date Prepared: 06/19/2020 1313h Arsenic 0.196 mg/L E200.8 0.000298 0.00200 0,2000 0.00157 97.1 75 -125 0.206 5.24 20 Beryllium 0.218 mg/L E200,8 0.000198 0.00200 0.2000 0 109 75 -125 0.22 0.925 20 Cadmium 0.201 mg/L E200.8 0.0000742 0.000500 0.2000 0 100 75 -125 0.199 0.910 20 Chromium 0.198 mg/L E200,8 0.00191 0.00200 0.2000 0 99.1 75 -125 0.206 3.66 20 Cobalt 0.200 mg/L E200.8 0.000300 0.00400 0.2000 0.00046 99.9 75 -125 0.207 3.17 20 Copper 0.203 mg/L E200,8 0.00166 0.00200 0.2000 0 102 75 -125 0.211 3.43 20 Iron 0.998 mg/L E200.8 0.0328 0.100 1.000 0 99.8 75 -125 1.04 3.77 20 Lead 0.201 mg/L E200.8 0.000448 0.00200 0.2000 0 IOI 75 -125 0.209 3.82 20 Molybdenum 0.216 mg/L E200.8 0.000652 0.00200 0.2000 0.00933 103 75 -125 0.218 1.12 20 Nickel 0.200 mg/L E200.8 0.000728 0.00200 0.2000 0.000968 99.6 75 -125 0.207 3.11 20 Selenium 0.188 mg/L E200 8 0.000508 0.00200 0.2000 0.00121 93.4 75 -125 0.197 4.56 20 Silver 0.197 mg/L E200.8 0.000232 0.00200 0.2000 0 98.7 75 -125 0.196 0.637 20 Thallium 0.195 mg/L E200.8 0.000390 0.00200 0.2000 0 97.4 75 -125 0.206 5.56 20 Report Date: 7/6/2020 Page 28 of 38 analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tr ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re•pub}ication of this report for any purpose other than for the addressee wiB be granted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2006528 Project: Annual Seeps & Springs 2020 Analyte Result -Lab Sample ID: 2006528-00IEMSD Dme Analy-Led: Test Code: 200.8-DIS Dale Prepared: Tin 103 Uranium 0.225 Zinc 1.02 Lab Sample ID: 2006528-002EMSD Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury 0.00344 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Units Method MDL Limit 07/01/2020 1324h 06/19/2020 1313h mg/L E200.8 0.00115 0.00400 1.000 mg/L E200.8 0.000176 0.00200 0.2000 mg/L E200,8 0.00418 0.00600 1.000 06/25/2020 92 lh 06/24/2020 1313h mg/L E245.I 0.0000396 0.0000900 0.003330 Tanner Holliday ME MSD Spike Ref. Amount %REC 0 103 0.0129 106 0 102 0 103 2 -Analyte concentration is loo high for accurate matrix spike recovery and/or RPD. Limits 75 -125 75 -125 75 -125 85 -115 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPO Limit 1.06 2.59 20 0.233 3.69 20 1.05 2.38 20 0.00349 I.JO 20 Qual Report Date: 7/6/2020 Page 29 of38 analyses applicable to the CWA, SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee, Privileges of subsequent use of ti- ne of trus company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact, This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2006528 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: 2006528-001 CDUP Date Analyzed: Test Code: TDS-W-2540C Total Dissolved Solids 1,450 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORl' Contact: Dept: QC Type: Reporting Amount Spiked Method MDL Limit Tanner Holliday WC DUP Spike Ref. Amount %REC 06/19/2020 1209h mg/L SM2540C 16.0 20.0 Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit 1480 2.18 5 Qua) Report Date: 7/6/2020 Page 30 of38 analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee, Privileges of subsequent use oftt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee wi11 be granted only on contact. This .Arne.dean W est ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2006528 Project: Annual Seeps & Springs 2020 Analyte Result Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: Tanner Holliday WC Method MDL Reporting Limit QC Type: LCS Amount Spiked Spike Ref. Amount %REC Lab Sample ID: LCS-RI40263 Date Analyzed: 06/25/2020 1058h Test Code: Chloride Fluoride Sulfate 300.0-W Lab Sample ID: LCS-Rl40020 Test Code: ALK-W-23208-LL Alkalinity (as CaC03) Lab Sample ID: LCS-70682 Test Code: NH3-W-350.l Ammonia (as N) Lab Sample ID: LCS-140246 Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) Lab Sample ID: LCS-Rl40103 Test Code: TDS-W-2540C Total Dissolved Solids 5.08 5.17 4.93 Date Analyzed: 250 Date Analyzed: Date Prepared: 1.87 Date Analyzed: 0.930 Date Analyzed: 186 mg/L E300.0 0.0565 mg/L E300.0 0.0240 mg/L E300.0 0.136 06/19/2020 808h mg/L SM2320B 0.369 06/25/2020 20 I Sh 06/25/2020 I 035h mg/L E350.l 0.0473 06/25/2020 1227h mg/L E353.2 0.00494 06/19/2020 1209h mg/L SM2540C 8.00 0.100 5.000 0.100 5.000 0.750 5.000 1.00 250.0 0.0500 2.000 0.0100 1.000 10.0 205.0 0 0 0 0 0 0 0 102 103 98.6 100 93.6 93.0 90.7 Limits 90 -110 90 -110 90-110 90 -110 90 -110 90 -110 80 -120 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPO Limit Amt %RPO Qual ReportDate: 7/6/2020 Page3lof38 analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC Confidential Business lnfonnation: This report is provided for the exclusive use of the addressee. Privileges of subsequent use oftt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYT:CAL LABORATOR1i::S Client: Energy Fuels Resources, Inc. Lab Set ID: 2006528 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: MB-Rl40263 Date Analyzed: Test Code: 300.0-W Chloride < 0.100 Fluoride < 0.100 Sulfate < 0.750 Lab Sample ID: MB-Rl40020 Date Analyzed: Test Code: ALK-W-23208-LL Bicarbonate (as CaC03) < 1.00 Carbonate (as CaC03) < 1.00 Lab Sample ID: MB-70682 Date Analyzed: Test Code: NH3-W-350. l Date Prepared: Ammonia (as N) < 0.0500 Lab Sample ID: MB-140246 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) < 0.0100 Lab Sample ID: MB-Rl40103 Date Analyzed: Test Code: TDS-W-2540C Total Dissolved Solids < 10.0 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Units Method MDL Limit 06/25/2020 104th mg/L E300.0 0.0565 0.100 mg/L E300,0 0.0240 0.100 mg/L E300,0 0.136 0.750 06/19/2020 808h mg/L SM2320B 0.369 1.00 mg/L SM2320B 0.369 1.00 06/25/2020 2009h 06/25/2020 1035h mg/L E350.l 0.0473 0.0500 06/25/2020 1225h mg/L E353 ,2 0.00494 0.0100 06/19/2020 1209h mg/L SM2540C 8.00 10.0 Tanner Holliday WC MBLK Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 7/6/2020 Page 32 of38 analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NE LAC protocols Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tJ- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact, This Ame.rican West ANALYTICAL LABORATORIES 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QCSUMMARX _REPORT Client: Energy Fuels Resources, Inc. Lab Set ID: 2006528 Contact: Tanner Holliday Dept: WC Project: Annual Seeps & Springs 2020 Analyte Lab Sample ID: 2006528-002BMS Test Code: Chloride Fluoride Sulfate 300.0-W Lab Sample ID: 2006528-00lBMS Test Code: ALK-W-23208-LL Alkalinity (as CaC03) Lab Sample ID: 2006528-002DMS Test Code: NH3-W-350.1 Ammonia (as N) Lab Sample ID: 2006528-00JDMS Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) Result Units Method Date Analyzed: 06/25/2020 1943h 430 mg/L E300.0 412 mg/L E300,0 848 mg/L E300.0 Date Analyzed: 06/19/2020 808h 2,940 mg/L SM2320B Date Analyzed: 06/25/2020 2055h Date Prepared: 06/25/2020 1035h 1.60 mg/L E350,l Date Analyzed: 06/25/2020 1246h 1.08 mg/L E353 .2 MDL 4.52 1.92 10.9 0.369 0.0473 0.00494 1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. QCType: MS Reporting Amount Spiked Spike Ref. Limit Amount %REC 8.00 400.0 25.8 IOI 8.00 400.0 0 103 60.0 400.0 469 94.7 1.00 2,500 450 99.8 0.0500 2.000 0 80.1 0.0100 1.000 0.0978 97.7 Limits 90 -110 90 -110 90 -110 80 -120 90 -110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual Report Date: 7/6/2020 Page 33 of38 analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee. Privileges of subsequent use ofti" ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West QC SUMMARY REPORT ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2006528 Dept: WC Project: Annual Seeps & Springs 2020 QC Type: MSD Reporting Amount Spiked Spike Ref. RPDRef. RPD Analyte Result Units Method MDL Limit Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 2006528-002BMSD Date Analyzed: 06/25/2020 1959h Test Code: 300.0-W Chloride 431 mg/L E300.0 4.52 8.00 400.0 25.8 IOI 90 -110 430 0.257 20 Fluoride 426 mg/L E300.0 1.92 8.00 400.0 0 106 90 -110 412 3.21 20 Sulfate 898 mg/L E300.0 10.9 60.0 400.0 469 107 90 -110 848 5.73 20 Lab Sample ID: 2006528-001 BMSD Date Analyzed: 06/19/2020 808h Test Code: ALK-W-23208-LL Alkalinity (as CaC03) 2,950 mg/L SM2320B 0.369 1.00 2,500 450 100 80 -120 2950 0.170 10 Lab Sample ID: 2006528-002DMSD Date Analyzed: 06/25/2020 2055h Test Code: NH3-W-350. I Date Prepared: 06/25/2020 I 035h Ammonia (as N) 1.63 mg/L E350.l 0.0473 0.0500 2.000 0 81.6 90 -110 1.6 1.79 10 Lab Sample ID: 2006528-00JDMSD Date Analyzed: 06/25/2020 1247h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.08 mg/L E353.2 0.00494 0.0100 1.000 0.0978 98.6 90 -110 1.08 0.834 IO 1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Report Date: 7/6/2020 Page 34 of38 analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols, Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2006528 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: LCS VOC-2 061920A Date Analyzed: Test Code: 8260D-W-DEN100 2-Butanone 23.6 Acetone 19.2 Benzene 20.3 Carbon tetrachloride 21.8 Chloroform 20.0 Chloromethane 14.4 Methylene chloride 18.1 Naphthalene 18.0 Tetrahydrofuran 18.6 Toluene 21.3 Xylenes, Total 65.8 Surr: l,2-Dichloroethane-d4 48.5 Surr: 4-Bromotluorobenzene 52.2 Surr: Dibromotluoromethane 52.2 Surr: Toluene-d8 52.7 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Method MDL Limit Tanner Holliday MSVOA LCS Spike Ref. Amount %REC 06/19/2020 709h µg/L SW8260D 1.22 20.0 20.00 0 118 µg/L SW8260D 2.76 20.0 20.00 0 96.2 µg/L SW8260D 0.147 1.00 20.00 0 102 µg/L SW8260D 0.859 1.00 20.00 0 109 µg/L SW8260D 0.166 1.00 20.00 0 99.9 µg/L SW8260D 0.802 1.00 20.00 0 72.2 µg/L SW8260D 0.381 1.00 20.00 0 90.3 µg/L SW8260D 0.704 1.00 20.00 0 90.2 µg/L SW8260D 0.436 1.00 20.00 0 92.8 µg/L SW8260D 0.285 1.00 20.00 0 106 µg/L SW8260D 0.575 1.00 60.00 0 110 µg/L SW8260D 50.00 97.0 µg/L SW8260D 50.00 104 µg/L SW8260D 50.00 104 µg/L SW8260D 50.00 105 Limits 74 -236 70 -350 80 -127 66 -143 79 -124 30 -149 65 -154 55 -128 59 -135 69 -129 66 -124 80 -136 85 -121 78 -132 81 -123 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPO Limit Qual Report Date: 7/6/2020 Page 35 of38 analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee, Privileges of subsequent use oftr ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee wi1l be granted only on contact This American 'West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2006528 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: MB VOC-2 061920A Date Analyzed: Test Code: 8260D-W-DEN100 2-Butanone <20.0 Acetone <20.0 Benzene < 1.00 Carbon tetrachloride < 1.00 Chloroform < 1.00 Chloromethane < 1.00 Methylene chloride < 1.00 Naphthalene < 1.00 Tetrahydrofuran < 1.00 Toluene < 1.00 Xylenes, Total < 1.00 Surr: l,2-Dichloroethane-d4 47.0 Surr: 4-Bromofluorobenzene 54.1 Surr: Dibromofluoromethane 46.2 Surr: Toluene-d8 53.2 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com QC _SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Method MDL Limit Tanner Holliday MSVOA MBLK Spike Ref. Amount %REC 06/19/2020 729h µg/L SW8260D 1.22 20.0 µg/L SW8260D 2.76 20.0 µg/L SW82600 0.147 1.00 µg/L SW8260D 0.859 1.00 µg/L SW8260D 0.166 1.00 µg/L SW8260D 0.802 1.00 µg/L SW8260D 0.381 1.00 µg/L SW8260D 0.704 1.00 µg/L SW82600 0.436 1.00 µg/L SW8260D 0.285 1.00 µg/L SW82600 0.575 1.00 µg/L SW8260D 50.00 94.0 µg/L SW8260D 50.00 108 µg/L SW8260D 50.00 92.3 µg/L SW8260D 50.00 106 Limits 80 -136 85 -121 78 -132 81 -123 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual Report Date: 7/6/2020 Page 36 of38 analyses applicable to the CWA, SOWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee, Privileges of subsequent use oftt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted on1y on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2006528 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: 2006528-00IAMS Date Analyzed: Test Code: 8260D-W-DEN100 2-Butanone 24.0 Acetone 20.0 Benzene 19.5 Carbon tetrachloride 20.9 Chloroform 19.6 Chloromethane 13.5 Methylene chloride 17.5 Naphthalene 19.8 Tetrahydrofuran 16.1 Toluene 20.6 Xylenes, Total 65.8 Surr: 1,2-Dichloroethane-d4 47.9 Surr: 4-Bromofluorobenzene 52.4 Surr: Dibromofluoromethane 51.8 Surr: Toluene-d8 53.0 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMML'\:R\7 REPORT Contact: Dept: QC Type: Reporting Amount Spiked Method MDL Limit Tanner Holliday MSVOA MS Spike Ref. Amount %REC 06/19/2020 950h µg/L SW8260D 1.22 20.0 20.00 0 120 µg/L SW8260D 2.76 20.0 20.00 0 100 µg/L SW8260D 0.147 1.00 20.00 0 97.5 µg/L SW8260D 0.859 1.00 20.00 0 105 µg/L SW8260D 0.166 1.00 20.00 0 97.9 µg/L SW8260D 0.802 1.00 20.00 0 67.6 µg/L SW8260D 0.381 1.00 20.00 0 87.4 µg/L SW8260D 0.704 1.00 20.00 0 99.1 µg/L SW8260D 0.436 1.00 20.00 0 80.6 µg/L SW8260D 0.285 1.00 20.00 0 103 µg/L SW8260D 0.575 1.00 60.00 0 110 µg/L SW8260D 50.00 95.8 µg/L SW8260D 50.00 105 µg/L SW8260D 50.00 104 µg/L SW8260D 50.00 I06 Limits 74 -236 70 -350 80 -127 66 -143 79 -124 30 -149 65 -154 55 -128 59 -135 69 -129 66 -124 80 -136 85 -121 78 -132 81 -123 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 7/6/2020 Page 37 of38 analyses applicable to the CW A, SDW A, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tr ne of this company or any member of its staff, or reproduction of this report in cormection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2006528 Project: Annual Seeps & Springs 2020 Analyte Result Lab Sample ID: 2006528-00IAMSD Date Analyzed: Test Code: 8260D-W-DEN100 2-Butanone 24.7 Acetone 21.3 Benzene 19.8 Carbon tetrachloride 22.1 Chloroform 20.1 Chloromethane 13.5 Methylene chloride 17.5 Naphthalene 20.5 Tetrahydrofuran 18.1 Toluene 21.3 Xylenes, Total 66.9 Surr: l ,2-Dichloroethane-d4 48.4 Surr: 4-Bromofluorobenzene 51.5 Surr: Dibromofluoromethane 52.0 Surr: Toluene-d8 52.9 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMM~~YllE_PORT Contact: Dept: QC Type: Reporting Amount Spiked Method MDL Limit Tanner Holliday MSVOA MSD Spike Ref. Amount %REC 06/19/2020 101 lh µg/L SW8260D 1.22 20.0 20.00 0 124 µg/L SW8260D 2.76 20.0 20.00 0 106 µg/L SW8260D 0.147 1.00 20.00 0 99.1 µg/L SW8260D 0.859 1.00 20.00 0 110 µg/L SW8260D 0.166 1.00 20.00 0 100 µg/L SW8260D 0.802 1.00 20.00 0 67.4 µg/L SW8260D 0.381 1.00 20.00 0 87.4 µg/L SW8260D 0.704 1.00 20.00 0 102 µg/L SW8260D 0.436 1.00 20.00 0 90.3 µg/L SW8260D 0.285 1.00 20.00 0 106 µg/L SW8260D 0.575 1.00 60.00 0 112 µg/L SW8260D 50.00 96.9 µg/L SW8260D 50.00 103 µg/L SW8260D 50.00 104 µg/L SW8260D 50.00 106 Limits 74 -236 70 -350 80 -127 66 -143 79 -124 30 -149 65 -154 55 -128 59 -135 69 -129 66 -124 80 -136 85 -121 78 -132 81 -123 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit 24 3.12 35 20 6.10 35 19.5 1.63 35 20.9 5.39 35 19.6 2.42 35 13.5 0.297 35 17.5 0 35 19.8 3.23 35 16.1 11.4 35 20.6 3.40 35 65.8 1.63 35 Qual Report Date: 7/6/2020 Page 38 of38 analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tr ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee wi11 be granted only on contact This American West Analytical Laboratories Rpt Emailed: UL Denison WORK ORDER Summary Work Order: 2006528 Due Date: 7/2/2020 Page 1 of 4 Client: Client ID: Project: Comments: Sample ID 2006528-00IA 2006528-0018 2006528-001 C 2006528-00ID 2006528-00lE 2006528-002A 2006528-002B 2006528-002C Printed: 06/18/20 13:25 Energy Fuels Resources, Inc. ENE300 Annual Seeps & Springs 2020 Contact: Tanner Holliday QC Level: III WO Type: Project QC 3 (no chromatograms). EDD-Denison. Email Group; Do not use "*R_" samples as MS/MSD.; Client Sample ID Westwater Seep .: .... , Ruin Spring Collected Date Received Date Test Code Matrix Sel Storage 6/16/2020 0845h 6/16/2020 1035h 6/18/2020 1100h 8260D-W-DENIOO Aqueous Test Group: 8260D-W-DEN 100; # of Analytes: 11 I# of Surr: 4 300.0-W 3 SEL Analytes: CL F S04 ALK-W-2320B-LL 2 SEL Ana[ytes: ALKB ALKC TDS-W-2540C 1 SEL Analytes: TDS NID-W-350.1 1 SEL Ana_lytes: NH3N NH3-W-PR N02/N03°W~353.2 1 S~L Analytes: N03N02N 200.7-DIS - 5 SEL Anolyres: CA MG K NA V 200.7-DIS-PR 200.8-DIS 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR HG-DW-DIS-245.1 1 SEL Anolytes: HG HG-DW-DIS-PR IONBALANCE 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 6/18/2020 1100h 8260D-W-DENIOO Aqueous Test Group: 8260D-W-DENJOO; # of Analytes: 11 I # ofSurr: 4 300.0-W 3 SEL Analytes: CL F S04 ALK-W-2320B-LL 2 SEL Analytes: ALKB ALKC TDS-W-2540C 1 SEL Anolytes: TDS VOCFridge df-wc df-wc df-tds df -no2/no3 & nh3 df -no2/no3 & nh3 df -no2/no3 &.-nb3 df-met df-met df-rnet df-met df-rnet df-rnet df-met VOCFridge df-wc df-wc df-tds LABORATORY CHECK: %M O RT O CN O TAT O QC O LUO 0 HOK___ HOK __ _ HOK___ COC Emailed ____ _ 3 3 WORK ORDER Summary Client: Energy Fuels Resources, Inc. Sample ID Client Sample ID Collected Date 2006528-002D Ruin Spring 6/16/2020 103 Sh 2006528-002E 2006528-00JA Cottonwood Spring 6/16/2020 0945h 2006528-00JB 2006528-00JC 2006528-00JD 2006528-00JE Work Order: 2006528 Due Date: 7/2/2020 Page2 of4 Received Date Test Code Matrix Sel Storage 6/18/2020 I IOOh NH3-W-350.I Aqueous 1 SEL Analytes: NH3N NH3-W-PR N02/N03-W-353.2 1 SEL Analytes: N03N02N 200.7-DIS 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR 200.8-DIS 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR HG-DW-DIS-245.1 1 SEL Analytes: HG HG-DW-DIS-PR IONBALANCE 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 6/18/2020 1100h 8260D-W-DENIOO Aqueous -Test Group: 8260D-W-DENJQO; # of Ana/ytes: 11 I # o/Surr: 4 300.0-W 3 SEL Analytes: CL F S04 ALK-W-2320B-LL 2 SEL Analytes: ALKB ALKC TDS-W-2540C I SEL Analytes: TDS NH3-W-350.l 1 SEL Analyte~: NH3N NH3-W-PR N02/N03-W-353.i I SEL Ana~tes: N03N02N 200.7-DIS 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR 200.8-DIS I 7 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR HG-DW-DIS-245.1 I SEL A11alytes: HG df -no2/no3 & nh3 df -no2/no3 & nh3 df -no2/no3 & nh3 df-met df-met df-met df-met df-met df-met df-met VOCFridge df-wc df-wc df-tds df -no2/no3 & nh3 df -no2/no3 & nh3 df -no2/no3 & nh3 df-met df-met df-met df-met df-met 3 Printed: 06/18/20 13:25 LABORATORY CHECK: %M O RT O CN O TAT O QC O LUO 0 HOK ___ HOK __ _ HOK___ COC Emailed _____ _ WORK ORDER Summary Client: Energy Fuels Resources, Inc. Sample ID Client Sample ID Collected Date 2006528-003E Cottonwood Spring 6/16/2020 094 Sh 2006528-004A Entrance Seep 6/16/2020 11 OSh 2006528-004B 2006528-004C 2006528-004D . · •· 2006528-004E •-. '*. ·"' .... :r , ..;,.-. • .;.- 2006528-00SA Back Spring 6/16/2020 0945h 2006528-00SB 2006528-00SC 2006528-00SD Work Order: 2006528 Due Date: 7/2/2020 Page3 of4 Received Date Test Code Matrix Sel Storage 6/18/2020 1100h HG-DW-DIS-PR Aqueous df-met IONBALANCE df-met 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 6/18/2020 1100h 8260D-W-DEN100 Aqueous VOCFridge Test Group_: 8260D-W-DEN100; # of Analytes: 11 1# ofSurr: 4 300.0-W df-wc 3 SEL Analytes: CL F S04 ALK-W-2320B-LL df-wc 2 SEL Analytes: ALKB ALKC TD8-W-2540C df-tds 1 SEL Analytes: TDS NH3-W-3SO.l df -no2/no3 & nh3 1 SEL Analytes: NH3N NH3-W-PR df -no2/no3 & nh3 N02/N03-W-353.2 df -no2/no3 & nh3 1 SEL Analytes: N03N02N ,, _,.., ... 0200.7-DIS ' · .. ~1·-~., .... · .. ,:;,.. df~met,. 5 SEL Analytes: CA MG K NA V 200.7-DIS:PR 200.8-DIS 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NJ SE AG TLSNUZN 200.8-DIS-PR HG-DW-DIS-245.1 1 SEL Analytes: HG HG-DW-DIS-PR IONBALANCE 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 6/18/2020 1100h 8260D-W-DEN100 Aqueous Test Group: 8260D-W-DENJOO; # of Analytes: 11 I# ofSurr: 4 300.0-W 3 SEL Analytes: CL F S04 ALK-W-2320B-LL 2 SEL Analytes: ALKB ALKC TDS-W-2540C 1 SEL Analytes: TDS NH3-W-3S0.1 1 SEL Analytes: NH3N df-met df-met df-met df-met df-met df-met VOCFridge df-wc df-wc df-tds df -no2/no3 & nh3 3 Printed: 06/18/20 13:25 LABORATORY CHECK: %M O RT O CN O TAT O QC O LUO 0 HOK ___ HOK __ _ HOK___ COC Emailed~---- WORK ORDER Summary Work Order: 2006528 Page 4 of 4 Client: Energy Fuels Resources, Inc. Due Date: 7/2/2020 Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 2006528-00SD Back Spring 6/16/2020 0945h 6/18/2020 1100h NH3-W-PR Aqueous df -no2/no3 & nh3 N02/N03-W-353.2 df -no2/no3 & nh3 1 SEL Analytes: N03N02N 2006528-00SE 200.7-DIS df-met 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR df-met 200.8-DIS df-met 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR df-met HG-DW-DIS-245.1 df-met 1 SEL Analytes: HG HG-DW-DIS-PR df-met IONBALANCE df-met 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 2006528-006A Trip Blank 6/16/2020 0845h 6/18/2020 11 OOh 8260D-W-DEN100 Aqueous VOCFridge 3 ... , Test Group: 8260D-W-DENJOO; # of Analytes: 11 I# o[Surr: 4 Printed: 06/18/20 13 :25 LABORATORY CHECK: %M O RT 0 CN O TAT D QC O LUO 0 HOK ___ HOK __ _ HOK___ COC Emailed'------- American West Analytical Laboratories 463 W. 3600 S. Salt Lake City, UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 L-~ Fax# (801) 263-8687 Email awal@awal-labs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: Email: kweinel@energyfuels.com; tholliday@energyfuels.com Project Name: Annual Seeps & Springs 2020 Project#: PO#: Sampler Name: Tanner Holliday Date Samole ID: Samoled Westwater Seep 6/16/2020 Ruin Spring 6/16/2020 Cottonwood Spring 6/16/2020 Entrance Seep 6/16/2020 5 ; Back spring 6/16/2020 6 I Trip Blank I I 8 8 (I I ! Relinquished oy..:...:J .1L. / /-_/_ A ""'('61urc ~ "'" • V 0nntNllrna: Tanner Hot""-· Re!inqulst,ed D)r. Slgnabn 'nn1Name: ~ellnqolsliedby: !Slnnatun:, P11/11Name: Relinqulsne4Dy. ""'naue "r1ntName: 6/16/2020 Dale; 61V/21l21 mme: 1100 Dale: ilmo: Dale: ilme: 0311):: ,tme: I Time Samoled 845 1035 945 1105 945 845 Rece1ve<1 Dy: Signature CHAIN OF CUSTODY All analysis will be conducted using NELAP accredited mett10ds and all dala will be reported using AWAL's slandard analyte lists and reporting limi1'1 (POL) unless specifK:aJly requested otherwise on this Chain or Custody and/or attached documenlatkm. QC Level: I Tum Around Time: Unless other arrangements have been made, signed reports will be emailed by 5:00 pm on 3 Standard lhe day they are due. X Include EDD: 0 LOCUS UPLOAD ::E c,j u EXCEL bQ bQ X Field Filtered For: ....,. ::r: ::E Dissolved Metals .... i:f Ii) ::E ~-"" C'l s:· cd ~ z For Compliance With: c::i &. ~-D NELAP 0 D RCRA o' C'l ;:i" > D CWA c::i ~ C c::i u ;::i 0 SOWA ....,. l') 0 -§' C) D ELAP/A2lA C) ... ~ u ~-C, 0 NLLAP ~ IJ) C) ~ Ill k rn (') C) 'iii u ~-D Non-Compliance t;j ... IJ) ~ °i D other: C, :t. •cf i t3' ~ !:2. C!:J t3' = Ill u 41 C) .. ·i:! 0 ~ 0 II IO C: <ii !') C) 0 ;)'; iii ,a .,· Cl) ~ C'l s 0 IJ) Ul OI ~ ~ :::; .ii rn Known Hazards C: II:; :t. d ~ rll 0 .!!! ... ... 0 :i IQ .. u a_ N ~ Ul i Ill < 0 & 0 E 0 ii a • "' 0 ., II:; 0 iS 0 > Samole Comments "' "' ... 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 3 w X Date: Special Instructions: ITime: 2-..aoCo S-~? AWAL Lab Sample Set# Page 1 of 1 r= ""· Laboratory Use Only Samples Wete; (A ;?S ,e~- 2 Amblento8 3 Temperatll'f> 0 · (JI ·c 4 Received Brokervleaking (Improperly SealG y N 5 <!J:J'ty PresGM!d y N Checke<I at bench y N 6 Rl!Cdvod Wlllin Holding Times () N Ir.cc Tape Was: 1 Preseol on Outer Package C) N NA ' 2 <'.!)""''"'" on Out..-Package Y N NA 3 Present on Sam pie G y N \ 4 Un!Jroken on Sample 0 Y N NA~ Dlscrepancles Between Sample Labels and COC Record? y C9 '"'ntName: Sample containers for metals were field filtered. See the R--~ .( c.Li . ().~Ir 'fir Ii_,, Analytical Scope of Work for Reporting Limits and voe analyte ~null.n --l~ ...d -1-7.:. . "I . ~ Time: list. ~-;; / I 0(\ Print Natr\O: ? IA-<.. /L..l - Recelvea Dy: { Date: Slanalute Time: Print Name: Received by: Date: Signature Time: Print Name: I Analysis Ammonia COD Cvanide Metals N02/N03 O&G Phenols Sulfide TKN TP04 Cr VI+ Procedure: Frequency: Preservation Check Sheet s le Set Ext amp: Preservative f 2 J 4-s pH <2 H2S04 \/_,-~5 V,,-1/ C ,/c. oH <2 H2S04 /' , I' , r r , oH>12NaOH _pH<2 HN03 i,.7 Yrs y:'.'..5 )~s Xi' 5 oH<2 H2S04 I/ '< v',., 1/ '7 '/.i..S Yes oH<2HCL I I I r I oH <2 H2S04 pH>9NaOH, Zn Acetate oH <2 H2S04 oH<2 H2S04 pH>9 <NRi)2S04 Pour a small amount of sample in the sample lid Pour sample from lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid doH 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + A # • The sample required additional preservative upon receipt. The sample was received unpreserved. The sample was received unpreserved and therefore preserved upon receipt. The sample pH was unadjustable to a pH < 2 due to the sample matrix. The sample pH was unadjustable to a pH> __ due to the sample matrix interference . Lab Set ID: pH Lot#: 260lr~.z? Ctj8"']_ m~-1 Laboratories LLC a member of The GEL Group INC PO Boxi0712 Ctm1estor1.SC29417 2040 Savage Road Cha~e$1on SC 29407 P 84~ 556.8171 F 84'.l766.1178 July 09, 2020 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: Analytical for Annual Seeps & Springs 2020 Work Order: 514075 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on June 19, 2020. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DW16138 Enclosures Page 1 of 18 SDG: 514075 _ .. ...,L,,..1--.......... 1 ............ Sincerely, ~~ Samuel Hogan for Julie Robinson Project Manager gel.com Page 2 of 18 SDG: 514075 Energy Fuels Resources (USA), Inc. Analytical for SDG: 514075 July 09, 2020 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 514075 Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on June 19, 2020 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following samples: Case Narrative: Laboratory ID 514075001 514075002 514075003 514075004 514075005 Client ID Wastewater Seep Ruin Spring Cottonwood Spring Entrance Seep Back Spring Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. Page 3 of 18 SDG: 514075 The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Page 4 of 18 SDG: 514075 ~~ Samuel Hogan for Julie Robinson Project Manager 5\4b15 . . r <".:: ·, >~~~~ . -· -.:-reNERGYFUELS RESOURCES Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: GEL Laboratories, LLC Contact: Tanner Holliday -=2-:-0-40~S-av_a_g_e-=R,....o __ a..,.d________ Ph: 435 678 2221 Charleston, SC 29407 tholllday@enerqyfuels.com (843) 556 8171 Chain of Custody/Sampling Analysis Request p . ro1ect Samp1ers N ame s amp ers s· 1gnature Annual Seeps & Springs L \11M1/J(, J!trf~-/(1 2020 Tanner Holliday V Time Sample ID Date Collected Collected Laboratory Analysis Requested Westwater Seep 6/16/2020 845 Gross Aloha Ruin Spring 6/16/2020 1035 Gross Alpha Cottonwood Sprina 6/16/2020 945 Gross Aloha Entrance Seep 6/16/2020 1105 Gross Alpha Back Sorlna 6/16/2020 945 Gross Aloha Comments: Please send report to Kathy Weinel at kweinel@.energyfuels.com Relinquished B :(Signature) .:J~ Tanner Holliday Relinquished By:(Signature) Page 5 of 18 SDG: 514075 Date/Time Received By:(Signature) 6/17/2020 /. / ~a,;,,, 1100 /A Date/Time Received By:(Signature) Date/Time c:. /l'l/2.o q'iS Date/Time I r.t:rm I l (·::!)()' s'i(J1 ·1oc: , ' , . ~ .11.IU,•.,u,;.;1, SAMPLE RECEIPT & REVIEW FORM Client: h~Ml SOG/Alt/COC/Wort, Order: h \4 o,c:.; Recci\'ctl By: Rl°lrlfJ.I; C:. Onie nccch·ccJ: &. • I q . 2.C · . -.\0 . Circkl •\11pli~bl~ Fed Ex Express FedEx Ground UPS Field Scn•ices Courier Other - Carrier anti Trncking Number IZ ll7 Y4V 12 qq5{) '-il7f Suspc.ctcd Hnurd lnformntion ~ C> 'IC Net Counts> IOOcpm on samples 1101 marked "rndioaetivc", co11tact the Radiation Safety Group for further investigation. > z Hazard Class Shipped: UNI/: A)Shio1x:d as a DOT Ma211rdous? .,,.. IH llN2910, Is the Rndioactivc Shijlment Sur,•cy Compliant? Yes Nn B) Did the client designate the samples are to be / COC nota'tiori or ra,Ho3i:tivc stickers <111 com3incrs e,1unl olicnt rtc~sun1ion. received as radioac.ti,·c? C) Did the RSO classify the samples as .,, Maximum Net Counts Obsct\·cd' (Obsc,.·cd Counts . Arca Bnckground Counts); _j2(_.cPi\l / mR/Mr rndionc1ivc? Cln.ssificd "" Rnll I Rud 2 Rad 3 D) Did the client designate samples ore lcoc lllll31 ion or hnZlird labels 011 containers cqiial client dc.,;ignntion . haz~rdons? .,, / U/ Dor E is yes, sclccl Hu211rds below. E) Did tho RSO idcntiJv oossible hn1.ards? PCB's Flammable Foreign Soil RCRA 1\sbcslos llcrylli11111 Olhcr: s~m11lc Rccci11t Criteria i'.l < 0 Conuncnls/Qunlificrs (Required for Non-Conforming Items) ;. z z 1 Shipping containers received intact and Circlo Applbbto. Scols brokon Dnm:i~ conu:iinct LC':,~inS containu Olhcr (do..,tibo) seol~d? /' 2 Cho in or custody documenls included / ~~i,\ ,t,'liooblo; Clicnl conwctcd ond provided COC COC crc.11cd upon rccciipt with shipment? 3 Samples requiring cold preservation ·y flrescrvntion Melhod: Wet Ice Ice Pucks Dry ice None Other: l r·v ~nll lcmperatnres arc rc~ordcd in Celsius -within (0 .5 6 deg. en• TEMP: 4 Daily check performed and passed on IR Tcm1tcrnturc Device Serial#: 'TR. L• Lq lemperniurc gun? ..,,, Sceondnry Tempen,ture Device Serial# (If Applicable): /' Circle ApplicQblc: Seols broken Dam:,.std con1ainct 1.c:iking. conlaincr Olhcr (Jc,c:ribo) 5 Sample containers intact and scaled? 6 Samples requiring chemical preservation / Sompto ID's ond l'on101nors Mfcclcd, at proper pH? If P,,..~,•r\-1! ... n ... .1 .. LJ I n•ll• If Y cs, are Encores or Soil Kits present for solic!s? Yes No NA (If i•cs, tnkc to VOA Freezer) Donny samples require Volatile Do liquid \101\ 1•ials contain acid prcscn·otion? Yes No NA (If unknown, select No) 7 Analysis? / /\re liquid VOA 1>iols free ofhcndspacc? Yes_ No_ N,\_ S:imp)c IO's and co111ni11crs nffcc1~d: ID's nnd tests affected: 8 Samples received within holding time? .;I# Sample ID's on COC match ID's on ID's nnd contnincrs nffcc1cd: 9 bottles? ./' 10 Dale & time on COC match date & time Circle /\ppticnblc: No doles on contnincrs No times on ~ontuiners COC missing info Other (describe) on bottles? Number of containers received match Circle Applicnblc: No contni11cr count on COC 01her (describe) 11 number indicated on COC? 12 Are sample containers idcntifioblc as CiEL ftrAv;.tA.t? 13 COC fonn is properly signed in Circle Applicable: Nol relinquished Other (dcscrirn:) relinauished/receivcd sections? Comments (Use Conlinunlion Fom, ifnccclcd): " '· PM (or PMA) review: lnitinls t\..\lZlv Dale {R/7.-Z, I 70 Pose _J_ of _L . GL-CHL-SR-001 Rev 6 Page 6 of 18 SDG: 514075 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 514075 Client SDG: 514075 Annual Seeps & Springs 2020 Project Manager: Project Name: Purchase Order: Package Level: EDD Format: Julie Robinson DNMI00106 Analytical for DW16138 LEVEL3 EIM_DNMI GELID Client Sample ID Client Sample Desc. 514075001 Wastewater Seep 514075002 Ruin Spring 514075003 Cottonwood Spring 514075004 Entrance Seep 514075005 Back Spring Collect Date & Time 16-JUN-20 08:45 16-JUN-20 10:35 16-JUN-20 09:45 16-JUN-20 11 :05 16-JUN-20 09:45 Work Order Due Date: 17-JUL-20 Package Due Date: 15-JUL-20 EDD Due Date: QA Due Date: IA®'Date: Receive Time # of Date & Time Zone Cont. 19-JUN-20 09:45 -2 1 19-JUN-20 09:45 -2 1 19-JUN-20 09:45 -2 1 19-JUN-20 09:45 -2 1 19-JUN-20 09:45 -2 1 17-JUL-20 17-JUL-20 18-JUL-20 Lab Matrix GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER Report Date: 09-JUL -20 Work Order: 514075 Page 1 of 2 Collector: C Prelogin #: 20190486669 Project Workdef ID: 1329132 SDG Status: Closed Logged by: Fax Daysto Prelog Lab Field Due Date Process CofC# Group QC QC 19 19 19 19 19 Client Sample ID Status Tests/Methods Product Reference Fax Date PM Comments Aux Data Receive Codes -001 Wastewater Seep -002 Ruin Spring -003 Cottonwood Spring -004 Entrance Seep -005 Back Spring REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid Product: GFCTORAL Workdef ID: 1461303 Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Samples: 001, 002, 003, 004, 005 Parmname Check: All parmnames scheduled properly CAS# Parmname Gross Radium Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha In Product Group? No Group Name: Client RDL or PQL & Unit Reporting Units pCi/L Group Reference: Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Parm Included Included Custom Function in Sample? in QC? List? REG y y No \r) r---0 -.:::t" ...... 0 Cl r:/1 00 ...... 4-< 0 r--- (1) 00 ~ p... GEL Laboratories LLC -Login Review Report Contingent Tests Action Login Requirements: Product Name Description Requirement Samples Include? Comments Peer Review by:. ___________ _ Work Order (SDG#), PO# Checked? ____ _ Report Date: 09-JUL-20 Work Order: 514075 Page 2 of 2 C of C signed in receiver location? _____ _ If) r--0 s::t" -If) ci Q 00 00 -4-4 0 00 ll.) ~ 0... List of current GEL Certifications as of 09 July 2020 State Certification Alabama 42200 Alaska 17-018 Alaska Drinking Water SC00012 Arkansas 88-0651 CLIA 42D0904046 California 2940 Colorado SC00012 Connecticut PH-0169 DoD ELAP/ ISO 17025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-15-00283,P330-15-00253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SOW A 90129 Kentucky Wastewater 90129 Louisiana Drinking Water LA024 Louisiana NELAP 03046 (AI33904) Maine 2019020 Maryland 270 Massachusetts M-SC012 Massachusetts PF AS Approv Letter Michigan 9976 Mississippi SC00012 Nebraska NE-OS-26-13 Nevada scooo 122020-1 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 2019-165 Pennsylvania NELAP 68-00485 Puerto Rico SCOOOl2 S. Carolina Radiochem 10120002 Sanitation Districts of L 9255651 South Carolina Chemistry 10120001 Tennessee TN 02934 TexasNELAP Tl04704235-20-17 UtahNELAP SCOOOl22020-32 Vermont VT87156 Virginia NELAP 460202 Washington C780 Page 9 of 18 SDG: 514075 Radiochemistry Technical Case Narrative Energy Fuels Resources SDG #: 514075 Product: GFPC, Total Alpha Radium, Liquid Analytical Method: EPA 903.0 Analytical Procedure: GL-RAD-A-044 REV# 10 Analytical Batch: 2013767 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 514075001 514075002 514075003 514075004 514075005 1204583696 1204583697 1204583698 1204583699 1204583700 Client Sample rdentification Westwater Seep Ruin Spring Cottonwood Spring Entrance Seep Back Spring Method Blank (MB) 514075005(Back Spring) Sample Duplicate (DUP) 514075005(Back Spring) Matrix Spike (MS) 514075005(Back Spring) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Miscellaneous Information Additional Comments The matrix spike and matrix spike duplicate, 1204583698 (Back SpringMS) and 1204583699 (Back SpringMSD), aliquots were reduced to conserve sample volume. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 10 of 18 SDG: 514075 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMI001 Energy Fuels Resources (USA), Inc. Client SDG: 514075 GEL Work Order: 514075 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. ReviewNalidation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: j~ ~ Name: Theresa Austin Date: 13 JUL 2020 Title: Group Leader Page 11 of 18 SDG: 514075 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QCSumma rl:'. Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Contact: Ms. Kathy Weinel Workorder: 514075 Parmname NOM Sample Qual Rad Gas Flow 3atch 2013767 QC!204583697 514075005 DUP Gross Radium Alpha u -0.00212 u Uncertainty +l-0.191 QC1204583700 LCS Gross Radium Alpha 570 Uncertainty QC 1204583696 MB Gross Radium Alpha u Uncertainty QC1204583698 514075005 MS Gross Radium Alpha 2300 u -0.00212 Uncertainty +l-0.191 QC1204583699 514075005 MSD Gross Radium Alpha 2300 u -0.00212 Uncertainty +l-0.191 Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product QC Units -0.0109 pCilL +l-0.189 635 pCi/L +I-7.47 -0.223 pCi/L +l-0.134 2360 pCilL +l-28.6 2130 pCi/L +l-27.3 RPO% NIA 10.4 A B BO C D F H K L M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Page 17 of 18 SDG: 514075 Reoort Date: July 13, 2020 REC% Rane Anlst NIA JXK3 111 (75%-125%) 103 (75%-125%) 92.8 (0%-20%) Page 1 of Date Time 07101/20 12:4 07101/20 12:4 07101/20 12:4, 07101/20 12:4 07101/20 12:4 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 514075 Parmname NOM Sam__pJe Qual __ QC Units RPO% __ R_E_C_"A_o __ R_a_nge Anlst M Matrix Related Failure NIA RPO or %Recovery limits do not apply. Nl ND NJ Q R u UI UJ UL X y /\ h See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPO of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of Date Time NI A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPO not applicable. I\ The Relative Percent Difference (RPO) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 18 of 18 SDG: 514075 TabE Quality Assurance and Data Validation Tables Table E-1 Holding Time Evaluation Cottonwood Entrance Back Spring West Water Required Holding Time Spring Seep (duplicate of Ruin Spring Seep Ruin Spring) Carbonate 14 days OK OK OK OK OK Bicarbonate 14 days OK OK OK OK OK Calcium 6 months OK OK OK OK OK Chloride 28 days OK OK OK OK OK Fluoride 28 days OK OK OK OK OK Magnesium 6 months OK OK OK OK OK Nitrogen-Ammonia 28 days OK OK OK OK OK Nitrogen-Nitrate 28 days OK OK OK OK OK Potassium 6 months OK OK OK OK OK Sodium 6 months OK OK OK OK OK Sulfate 28 days OK OK OK OK OK pH (s.u.) NIA OK OK OK OK OK TDS 7 days OK OK OK OK OK 6 months (except mercury which is 28 Metals days) OK OK OK OK OK Radiologies 6 months OK OK OK OK OK VOCS (including THF) 14 days OK OK OK OK OK * -Corral Spring, and Corral Canyon were all dry and no samples were collected. E-2 Laboratory Receipt Temperature Check '.\\\1 ork 0Fcl :r Nw,nhel'hLmri Se1 Jll) tl@e-i!J)l~ 'Femp 2003627 2.0°c GEL -508151 NIA AW AL -2006528 0.6°C GEL-514075 NIA NI A = These shipments contained samples for the analysis of Gross Alpha only. Per Table 1 in the approved QAP, samples submitted for Gross Alpha analyses do not have a sample temperature requirement. E-3: Analytical Method Check -Routine Samples Parameter QAP/Pevmit Method Method Used by Lab Ammonia ( as N) A4500-NH3 G or E350. l E350.l Nitrate+ Nitrite (as N) E 353.1 or E353.2 E353.2 Metals E 200.7 or E200.8 E200.7, E200.8 Mercury E200.7 or E200.8 or E245.l E245.l Gross Alpha E900.0 or E900. l or E903.0 E903.0 voes SW8260B or SW8260C or SW8260D SW8260D Chloride A4500-Cl B, A4500-Cl E, or E300.0 E300.0 Fluoride A4500-F C or E300.0 E300.0 Sulfate A4500-S04 E or E300.0 E300.0 TDS A2540C A2540C Carbonate as C03, Bicarbonate as HC03 A2320B A2320B Calcium, Magnesium, Potassium, Sodium E200.7 E200.7 E-4 Reporting Limit Evaluation Parameter Permit-Specified RL Ammonia (as N) 25 mg/L Nitrate + Nitrite (as N) 10 mg/L Metals ug/L Arsenic 50 Beryllium 4 Cadmium 5 Chromium 100 Cobalt 730 Copper 1300 Iron 11000 Lead 15 Manganese 800 Mercury 2 Molybdenum 40 Nickel 100 Selenium 50 Silver 100 Thallium 2 Tin 17000 Uranium 30 Vanadium 60 Zinc 5000 Gross Alpha 15 VOCsug/L Acetone 700 Benzene 5 Carbon tetrachloride 5 Chloroform 70 Chloromethane 30 MEK 4000 Methylene Chloride 5 Naphthalene 100 Tetrahydrofuran 46 Toluene 1000 Xylenes 10000 Major Ions mg/L Chloride l Fluoride 4 Sulfate 1 TDS 10 Carbonate as C03, Bicarbonate as HC03 Not Specified Calcium, Magnesium, Potassium, Sodium Not Specified All analyses were reported to the required RLs unless noted in the text. E-5: Trip Blank Evaluation Blank Sample Date Analyte Re.suit {ug/L) 2-Butanone ND Acetone ND Benzene ND Carbon tetrachloride ND Chloroform ND 2003627 3/25/2020 Chloromethane ND Methylene chloride ND Naphthalene ND Tetrahydrofuran ND Toluene ND Xylenes, Total ND 2-Butanone ND Acetone ND Benzene ND Carbon tetrachloride ND Chloroform ND 2006528 6/16/2020 Chloromethane ND Methylene chloride ND Naphthalene ND Tetrahydrofuran 3.83 Toluene ND Xylenes, Total ND E-6 Duplicate Sample Relative Percent Difference Back Spring Major Ions (mg/I) Cottonwood Spring (Duplicate of RPD% Cottonwood Spring) Carbonate <1.00 <1.00 N/C Bicarbonate 280 284 1.4 Calcium 120 124 3.3 Chloride 146 147 0.7 Fluoride 0.233 0.240 3.0 Magnesium 32.9 33.7 2.4 Nitrogen-Ammonia <0.0500 <0.0500 N/C Nitrogen-Nitrate <0.100 <0.100 N/C Potassium 7.14 7.23 1.3 Sodium 273 282 3.2 Sulfate 417 424 1.7 TDS 860 1280 39.3 Metals (ug/1) Arsenic <5.0 <5.0 N/C Beryllium <0.5 <0.5 N/C Cadmium <0.5 <0.5 NIC Chromium <25 <25 N/C Cobalt <10 <10 NIC Copper <10 <10 N/C Iron <30 <30 NIC Lead <1.0 <1.0 N/C Manganese <10 <10 N/C Mercury <0.5 <0.5 N/C Molybdenum <10 <10 N/C Nickel <20 <20 N/C Selenium <10 <10 N/C Silver <10 <10 NIC Thallium <0.5 <0.5 N/C Tin <100 <100 N/C Uranium 10.5 10.7 1.9 Vanadium <15 <15 NIC Zinc <10 <10 N/C Radiologies (pCi/1) Gross Alpha <1.00 <1.00 NIC voes (ug/L) Acetone <20.0 <20.0 N/C Benzene <1.00 <1.00 N/C Carbon tetrachloride <1.00 <1.00 NIC Chloroform <1.00 <1.00 N/C Chloromethane <1.00 <1.00 N/C MEK <20.0 <20.0 NIC Methylene Chloride <1.00 <1.00 N/C E-6 Duplicate Sample Relative Percent Difference 11 Bnek >Ping M}ljl)11 !funs, (mg,il~ Cottou:wr;iod Sprilng ~uulicate of RFD ~ otrto11~'\lootl Spring) Naphthalene <1.00 <1.00 N/C Tetrahydrofuran <1.00 <1.00 N/C Toluene <1.00 <1.00 N/C Xylenes <1.00 <1.00 N/C N/C = Not Calculated Per Lhe approved QAP, an RPO greater than 20% is acceplable if the reponed results are less than 5 times the RL. These results are provided for informalion only. * Duplieate ehec.k repo.-ted for gr-0s alpha minus 'RN and U are not %RPO. ~aleulated values are based on the fonml.ila in the appr<:>ved OWDP and QA:.P. RPD exceed. the QAP Umit of20%. E-7 Radiologies Counting Error Gress Alpha C0unting Gi:0s Alpha minu Rn&U Er.r0r·$; Within Sample ID minu Rn&U PJJecision (±) 20% GWQS GWQS Gottonwcmd Spring <1.0 0.209 NIA 15 NIA EntFance See~ <1.0 0.453 NIA 15 NIA Back Spring ( auplicate of Cottonwodd Spring) <1.0 0.191 NIA 15 NIA Ruin Spring <1.0 0.231 NIA 15 NIA Westwater Seep <1.0 0.191 NIA 15 NIA Westwater Seep <1.0 0.300 NIA 15 NIA NI A -The sample results are non-detect and the QAP required checks are not applicable. E-8: Laboratory Matrix QC Matrix Spike % Recovery Comparison MS MSO REC RPO Lab Report Well Analyte %REC %REC Range RPO LIMIT 2003627 Westwater Seep Ammonia (as N) 83.6 67.8 90-110 20 IO 2006528 Westwater Seep Calcium* NC NC 70 -130 NC 20 2006528 Westwater Seep Sodium* NC NC 70 -130 NC 20 2006528 Ruin Spring Ammonia (as N) 80.1 81.6 90-110 1.6 IO * Recovery was not calculated as the analyte level in the sample was greater than 4 times the spike amount. Laboratory Duplicate % Recovery Comparison Lat> ample Duplieale II Result Result LabRegQrt Well Analyte (mg/L) (mg/L) RPil> % RPD Range o/o 2003627 Westwater Seep TDS 1070 1200 11.3 5 Surrogate % Recovery All surrogate recoveries were within the laboratory established acceptance limits. Method/Laboratory Reagent Blank detections All method blank results were within the laboratory established acceptance limits. TabF CSV Transmittal Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Goble, Kathy Weinel Thursday, February 11, 2021 11 :08 AM Phillip Goble 'Dean Henderson'; David Frydenlund; Terry Slade; Logan Shumway; Scott Bakken Transmittal of CSV Files White Mesa Mill 2020 Annual Seeps and Springs Monitoring 508151.csv; 514075.csv; 2003627-report-EDD.csv; 2006528-report-EDD.csv Attached to this e-mail are the electronic copies of laboratory results for the annual seeps and springs monitoring conducted at the White Mesa Mill during 2020, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel 'eF -·-Energy Fuels Resources (USA) Inc. Kathy Weinel Quality Assurance M: nager t: 303.389.4134 I t: 303.389.4125 225 Union Blvd., Suite 600 Lakewood, CO 80228 http://www.energyfuels.com This e-mail is intended for the exclusive use of person(s) mentioned as the recipient(s). 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