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HomeMy WebLinkAboutDRC-2020-001382 - 0901a06880bc5cb5DI3C-202,0- 001381 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www.energyfuels.corn it 'ENERGY FUELS VIA Express Delivery January 14, 2020 Div of Waste Management and Radiation Control JAN 1 7 2020 Mr. Ty L. Howard Director of Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144880 Salt Lake City, UT 84116 Re: Transmittal of Annual Seeps and Springs Monitoring Report Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr. Howard: Enclosed are two copies of the White Mesa Uranium Mill Annual Seeps and Springs Monitoring Report for 2019 as required by the Groundwater Quality Discharge Permit UGW370004, as well as two CDs that contain a word searchable electronic copy of this report. If you should have any questions regarding this report please contact me at 303-389-4134. Yours very truly, ENERGY FUELS RESOU CES (USA) INC. Kathy Weinel Quality Assurance Manager CC: David Frydenlund Scott Bakken Paul Goranson Terry Slade VIA Express Delivery January 14, 2020 Mr. Ty L. Howard Director of Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144880 Salt Lake City, UT 84116 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www.encrgyfu I . m Re: Transmittal of Annual Seeps and Springs Monitoring Report Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr. Howard: Enclosed are two copies of the White Mesa Uranium Mill Annual Seeps and Springs Monitoring Report for 2019 as required by the Groundwater Quality Discharge Permit UGW370004, as well as two CDs that contain a word searchable electronic copy of this report. If you should have any questions regarding this report please contact me at 303-389-4134. Yours very truly, ENERGY FUELS REsou CE (USA) INC. Kathy Weinel Quality Assurance Manager CC: David Frydenlund Scott Bakken Paul Goranson Terry Slade White Mesa Uranium Mill 2019 Annual Seeps and Springs Sampling Report State of Utah Groundwater Discharge Permit No. UGW370004 Prepared by: ~RGYFUELS Energy Fuels Resources (USA) Inc. 225 Union Blvd., Suite 600 Lakewood, CO 80228 January 4, 2020 Contents 1.0 INTRODUCTION .................................................................................................................................. I 2.0 SAMPLING EVENTS ............................................................................................................................. I 2.1 March 2019 Sampling ......................................................................................................................... I 2.2 June 2019 Sampling ............................................................................................................................ I 2.3 Repeat Visits to Dry Seeps and Springs .............................................................................................. 1 2.4 Sampling Procedures .......................................................................................................................... 2 2.5 Field Data ............................................................................................................................................ 3 2.6 Field QC Samples ............................................................................................................................... 3 3.0 SEEPS AND SPRINGS SURVEY AND CONTOUR MAP ................................................................. 3 4.0 QUALITY ASSURANCE AND QUALITY CONTROL ..................................................................... .4 4.1 Laboratory Results .............................................................................................................................. 4 4.2 DATA EVALUATION ...................................................................................................................... 4 4.3 Adherence to Sampling Plan and Permit Requirements ..................................................................... 5 4.4 Analyte Completeness Review ........................................................................................................... 5 4.5 Data Validation ................................................................................................................................... 5 4.5 .1 Field Data QA/QC Evaluation ..................................................................................................... 5 4.5.2 Holding Time Evaluation ............................................................................................................. 5 4.5.3 Laboratory Receipt Temperature Check ...................................................................................... 5 4.5.4 Analytical Method Check ............................................................................................................ 6 4.5.5 Reporting Limit Evaluation ........................................................................................................... 6 4.5.6 Trip Blank Evaluation .................................................................................................................. 6 4.5.7 QA/QC Evaluation for Sample Duplicates .................................................................................. 6 4.5.8 Radiologies Counting Error ......................................................................................................... 7 4.5.9 Laboratory Matrix QC Evaluation ............................................................................................... 7 5.0 EVALUATION OF ANALYTICAL DATA .......................................................................................... 8 5.1 Evaluation of Analytical Results ......................................................................................................... 9 5.1.1 RuinSpring .................................................................................................................................. 9 5 .1.2 Cottonwood Spring ...................................................................................................................... 9 5 .1.3 Westwater Seep .............................................................................. ·-· ............................................ 9 5.1.4 Entrance Spring .......................................................................................................................... 10 6.0 CORRECTIVE ACTION REPORT ..................................................................................................... 10 6.1 Assessment of Corrective Actions from Previous Period ................................................................. 10 7.0 ELECTRONIC DATA FILES AND FORMAT ................................................................................... 10 8.0 SIGNATURE AND CERTIFICATION ............................................................................................... 12 ii Table 1 Table 2A Table 2B Table 2C Table 2D LIST OF TABLES Summary of Seeps and Springs Sampling Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Ruin Spring Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Cottonwood Seep Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Westwater Seep Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Entrance Spring INDEX OF TABS Tab A Seeps and Springs Field Data Sheets and Photographic Documentation Tab B Field Parameter Measurement Data Tab C Survey Data and Contour Map Tab D Analytical Laboratory Data Tab E Quality Assurance and Data Validation Tables E-1 Holding Time Evaluation E-2 Laboratory Receipt Temperature Check E-3 Analytical Method Check E-4 Reporting Limit Evaluation E-5 Trip Blank Evaluation E-6 QA/QC Evaluation for Sample Duplicates E-7 Radiologies Counting Error E-8 Laboratory Matrix QC Evaluation Tab F Comma Separated Values Transmittal 111 AWAL DR DWMRC EFRI GEL GWQS LCS Mill MS MSD Permit QA QAP QC RPD TDS voes ACRONYM LIST American West Analytical Laboratory Dry Ridge Piezometers Utah Division of Waste Management and Radiation Control Energy Fuels Resources (USA) Inc. GEL Laboratories, Inc. Groundwater Quality Standard Laboratory Control Spike White Mesa Mill Matrix Spike Matrix Spike Duplicate State of Utah Groundwater Discharge Permit No. UGW370004 Quality Assurance Groundwater Monitoring Quality Assurance Plan Quality Control Relative Percent Difference Total Dissolved Solids Volatile Organic Compounds iv ANNUAL SEEPS AND SPRINGS SAMPLING REPORT 1.0 INTRODUCTION This is the 2019 Annual Seeps and Springs Sampling Report for the Energy Fuels Resources (USA) Inc. ("EFRI") White Mesa Mill (the "Mill"), as required under Part I.F.7 of the Mill's State of Utah Groundwater Discharge Permit No. UGW370004 (the "Permit") and the Mill's Sampling and Analysis Plan for Seeps and Springs, Revision: 2, July 8, 2016 (the "Sampling Plan"). The Sampling Plan for Seeps and Springs was revised in July 2016 to incorporate changes requested by the Division of Waste Management and Radiation Control ("DWMRC"). The Sampling Plan for Seeps and Springs, Revision: 2, July 8, 2016 was approved by DWMRC by letter dated August 8, 2016. 2.0 SAMPLING EVENTS Seeps and springs which were identified near the Mill in the 1978 Environmental Report (Plate 2.6-10, Dames and Moore, January 30, 1978) are to be sampled annually in accordance with the Sampling Plan and Part 1.E.6 of the Permit. The Sampling Plan specifies the following sample locations: Corral Canyon Seep, Corral Springs, Ruin Spring, Cottonwood Seep, Westwater Seep and Entrance Spring (also referred to as Entrance Seep). 2.1 March 2019 Sampling In accordance with the DWMRC-approved Sampling Plan, once per calendar quarter, Westwater Seep, Corral Canyon Seep and Corral Springs are visited to determine if there is any water for sampling. If sufficient water is present, a sample is collected and no further visits are completed for the year. Westwater Seep, Corral Canyon Seep and Corral Springs were visited on March 20, 2019. No water was present for sampling during the March 20, 2019 site visit. On March 27, water was noted at Westwater seep and a sample was collected. Per the DWMRC-approved Sampling Plan, no further visits were made to Westwater seep in 2019. 2.2 June 2019 Sampling In accordance with the Permit and the Sampling Plan, DWMRC was notified of the sampling. The DWMRC representative was present for this sampling event. On June 11, 2019, EFRI collected seeps and springs samples from Cottonwood Seep, Ruin Spring, Entrance Seep, and Back Spring (duplicate of Ruin Spring). The DWMRC representative collected a "split" sample on June 11, 2019 from the EFRI sampling equipment, using sample containers he provided. Corral Canyon Seep and Corral Springs were dry throughout 2019. 2.3 Repeat Visits to Dry Seeps and Springs. The initial 2019 visit of Corral Canyon Seep and Corral Springs, was conducted in March 2019. Corral Canyon Seep and Corral Springs, were dry during the March 2019 visit, could not be sampled, and did not warrant development attempts with limited hand tool excavation at that time. During the June 11, 2019 sampling event, Corral Canyon Seep and Corral Springs were dry, could not be sampled, and did not warrant development attempts with limited hand tool excavation at that time. Additional visits were made to Corral Canyon Seep and Corral Springs in August 2019 and October 2019. The additional two visits to Corral Canyon Seep and Corral Springs did not indicate any changes; i.e., there was no indication that development attempts would be successful. As previously noted, a sample was collected from Westwater Seep on on March 27, 2019 because water was present. The data from the March and June sampling events are included as Attachment D in this report. 2.4 Sampling Procedures Samples were collected and analyzed for the parameters listed in Table 2 of the Permit. Samples were collected from the locations indicated in Table 1. Sampling procedures for each seep or spring are determined by the site location and access. The DWMRC-approved sampling procedures for seeps and springs at the Mill are contained in the Sampling Plan. Samples collected under this plan were collected either by direct collection which involves collecting the sample directly into the sample container from the surface water feature or from spring out-flow, or by using a stainless steel ladle to collect water until a sufficient volume is contained in the ladle for transfer to the sample bottle. Filtered parameters are pumped through a 0.45 micron filter prior to delivery to the sample bottle. Ruin Spring In the case of Ruin Spring, sample bottles for the analytes collected during the June sampling event (except gross alpha and heavy metals) were filled directly from the spring out-flow which is a pipe. Samples for heavy metals and gross alpha were collected by means of a peristaltic pump and delivered directly to the sample containers through a 0.45 micron filter. The appropriate preservatives for the analytical technique were added to the samples. Westwater Seep For Westwater Seep, all of the sample containers were filled by means of a peristaltic pump and delivered directly to the sample containers. Samples for heavy metals and gross alpha were collected by means of a peristaltic pump and delivered directly to the sample containers through a 0.45 micron filter. The appropriate preservatives for the analytical technique were added to the samples. Cottonwood Seep and Entrance Spring Cottonwood Seep and Entrance Spring were "developed" prior to the sampling event by Field Personnel. Development was completed by removing surrounding vegetation and clearing the sampling location in the spring or seep area. The sample containers were filled by means of a peristaltic pump and delivered directly to the sample containers. In the case of the samples for heavy metals and gross alpha, the samples were delivered by a peristaltic pump directly to the 2 sample containers through a 0.45 micron filter. The samples were preserved by the addition of the appropriate preservative for the analytical technique. The tubing on the peristaltic pump that comes into contact with the sample water was disposed of between each sampling. As a result, no equipment required decontamination, and no rinsate samples were collected. 2.5 Field Data Attached under Tab A are copies of the field data sheets recorded in association with the June and October seeps and springs monitoring events. Photographic documentation of the sampling sites is also included in Tab A. Sampling dates are listed in Table 1 and field parameters collected during the sampling program are included in Tab B. 2.6 Field QC Samples The field Quality Control ("QC") samples generated during this sampling event included one duplicate per sampling event and one trip blank per shipment to each laboratory which received samples for VOCs. The duplicate samples (Back Spring) were submitted blind to the analytical laboratory. As previously stated, no rinsate blanks were collected during this sampling event as only disposable equipment was used for sample collection. 3.0 SEEPS AND SPRINGS SURVEY AND CONTOUR MAP Part I.F.7(c) of the Permit requires that a water table contour map that includes the elevations for each well at the facility and the elevations of the phreatic surfaces observed for each of the seeps and springs sampled be submitted with this annual report. Tab C includes two contour maps. The contour map labeled C-1 shows the water table without the water level data associated with the dry ridge ("DR") investigation piezometers. The contour map labeled C-2 shows the water table with the water level data associated with the DR investigation piezometers. It is important to note that Cottonwood Seep is not included in any of the perched water level contouring, because there is no evidence to establish a hydraulic connection between Cottonwood Seep and the perched water system. Cottonwood Seep is located near the Brushy Basin Member/Westwater Canyon Member contact, approximately 230 feet below the base of the perched water system defined by the Burro Canyon Formation/Brushy Basin Member contact. The stratigraphic position of Cottonwood Seep indicates that its elevation is not representative of the perched potentiometric surface. Exclusion of the Cottonwood Seep from water level contouring is consistent with previous submissions. The contour map includes the corrected survey data from December 2009 as discussed below. Part I.F.7 (g) of the Permit requires that survey data for the seeps and springs be collected prior to the collection of samples. DRC previously clarified that the requirement to submit survey data applies only to the first sampling event and not on an annual basis. The December 2009 and July 2010 seeps and springs survey data shown in Tab C will be used for reporting where seeps and springs locations and elevations are relevant. 3 A full discussion of the survey data and the hydrogeology of seeps and springs at the margins of White Mesa in the vicinity of the Mill and the relationship of these seeps and springs to the hydrogeology of the site, in particular to the occurrence of a relatively shallow perched groundwater zone beneath the site, is contained in Hydrogeology of the Perched Groundwater Zone and Associated Seeps and Springs Near the White Mesa Uranium Mill Site, dated November 12, 2010, prepared by Hydro Geo Chem, Inc. and submitted to the Director on November 15, 2010. Additional information is also contained in the Second Revision Hydrogeology of the Perched Groundwater Zone in the Area Southwest of the Tailings Cells White Mesa Mill Site, dated November 7, 2012, prepared by Hydro Geo Chem, Inc. and submitted to the Director on November 7, 2012. 4.0 QUALITY ASSURANCE AND QUALITY CONTROL 4.1 Laboratory Results Analytical results are provided by the Mill's two contract analytical laboratories GEL Laboratories, Inc., ("GEL") and American West Analytical Laboratory ("AW AL"). The laboratories utilized during this investigation were certified under the Environmental Lab Certification Program administered by UDEQ Bureau of Lab Improvement for the analyses they completed. The analytical data as well as the laboratory Quality Assurance ("QA")/QC summaries are included under Tab D. 4.2 DATA EVALUATION The Permit requires that the annual seeps and springs sampling program be conducted in compliance with the requirements specified in the Mill's approved White Mesa Uranium Mill Groundwater Monitoring Quality Assurance Plan ("QAP"), the approved Sampling Plan and the Permit. To meet this requirement, the data validation completed for the seeps and springs sampling program verified that the program met the requirements outlined in the QAP, the Permit and the approved Sampling Plan. The Mill QA Manager performed a QA/QC review to confirm compliance of the monitoring program with requirements of the Permit and the QAP. As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and quality control review of laboratory data methods and data. Identification of field QC samples collected and analyzed is provided in Section 4.5.1. Discussion of adherence to the Sampling Plan is provided in Section 4.3. Analytical completeness review results are provided in Section 4.4. The steps and tests applied to check laboratory data QA/QC are discussed in Sections 4.5.1 through 4.5.9 below. The analytical laboratories have provided summary reports of the analytical QA/QC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference certification and reporting protocol. The analytical laboratory QA/QC Summary Reports, including copies of the Mill's Chain of Custody and Analytical Request Record forms for each set of analytical results, follow the analytical results under Tab D. Results 4 of the review of the laboratory QA/QC information are provided under Tab E and discussed in Section 4.5 below. 4.3 Adherence to Sampling Plan and Permit Requirements On a review of adherence by Mill personnel to the Permit, the QA Manager observed that QA/QC requirements established in the Permit and the QAP were met and that the requirements were implemented as required except, as noted below. The Permit only requires the measurement of the field parameters pH, conductivity and temperature. Field parameter measurements collected during this sampling event included pH, conductivity, temperature, redox potential, and turbidity. 4.4 Analyte Completeness Review The analyses required by the Permit Table 2 were completed. 4.5 Data Validation The QAP and the Permit identify the data validation steps and data quality control checks required for the seeps and springs monitoring program. Consistent with these requirements, the QA Manager performed the following evaluations: a field data QA/QC evaluation, a receipt temperature check, a holding time check, an analytical method check, a reporting limit check, a trip blank check, a QA/QC evaluation of sample duplicates, a gross alpha counting error evaluation and a review of each laboratory's reported QA/QC information. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab E. 4.5.1 Field Data QA/QC Evaluation The QA Manager performs a review of field recorded parameters to assess their adherence with QAP and Permit requirements. The assessment involved review of the Field Data sheets. Review of the Field Data Sheets noted that the requirements for field data collection were met. 4.5.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided under Tab E. The samples were received and analyzed within the required holding time. 4.5.3 Laboratory Receipt Temperature Check Chain of Custody sheets were reviewed to confirm compliance with the sample receipt requirements specified in the QAP. Sample receipt temperature checks are provided under Tab E. The samples were received within the QAP required temperature limit. 5 4.5.4 Analytical Method Check The analytical methods reported by both laboratories were checked against the required methods specified in Table 1 of the QAP. Analytical method check results are provided in Tab E. 4.5.5 Reporting Limit Evaluation Reporting limits utilized by the laboratory were required to be equal to or lower than the GWQSs set out in Table 2 of the Permit. For Total Dissolved Solids ("TDS"), sulfate and chloride, for which Ground Water Quality Standards are not set out in Table 2 of the Permit, reporting limits specified in Part 1.E.6.e).(l) were used. Those reporting limits are 10 mg/L for TDS, and 1 mg/L for Sulfate and Chloride. The analytical method reporting limits reported by both laboratories were checked against the reporting limits specified in the Permit. Reporting limit evaluations are provided in Tab E. All analytes were measured and reported to the required reporting limits except the sample results that had the reporting limit raised due to sample dilution necessary to accommodate the analyte concentrations in the samples. In all cases the reported value for the analyte was higher than the increased detection limit. 4.5.6 Trip Blank Evaluation The trip blank results were reviewed to identify any blank contamination. Trip blank evaluation is provided in Tab E. The trip blank results associated with the samples were less than reporting limit for the voes. 4.5. 7 QA/QC Evaluation for Sample Duplicates Section 9 .1.4 a) of the QAP states that the Relative Percent Difference ("RPD") will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results (described as activities in the QAP) are less than 5 times the required detection limit. This standard is based on the United Stated Environmental Protection Agency Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for duplicate pairs for the anal ytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits; however, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPO is greater than 20%. RPDs are also only calculated when both the sample and the duplicate report a detection for any given analyte. If only one of the pair reports a detection, the RPD cannot be calculated. The additional duplicate information is provided for information purposes. All duplicate results were within 20% RPD except for magnesium in the duplicate pair Ruin Spring/Back Spring. The magnesium RPD was greater than 20%, however the sample and duplicate results reported for Ruin Spring/Back Spring were not five times greater than the RLs, and, as such, the deviation from the 20% RPD requirement is acceptable. The duplicate evaluation is provided in Tab E. 6 4.5.8 Radiologies Counting Error Section 9.14 of the QAP requires that all gross alpha analysis reported with an activity equal to or greater than the Groundwater Compliance Limits set out in the Permit (for the seeps and springs samples the Groundwater Quality Standards ["GWQS"] will be used), shall have a counting variance that is equal to or less than 20% of the reported activity concentration. An error term may be greater than 20% of the reported activity concentration when the sum of the activity concentration and error term is less than or equal to the GWQS. Section 9.4 of the QAP also requires a comparability check between the sample and field duplicate sample results utilizing the formula provided in the text. All radiological results were reported were within acceptance limits. Results of routine radiologic sample QC are provided under Tab E. 4.5.9 Laboratory Matrix QC Evaluation Section 9.2 of the QAP requires that the laboratory's QA/QC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate analytical laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, EFRI's QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided under Tab E. The lab QA/QC results from both GEL and AW AL met these requirements except as described below. A number of the seeps and springs samples had the reporting limit raised due to matrix interference and/or sample dilution. In all cases where the detection limit was increased, the concentration for the analyte was higher than the increased detection limit. The check samples included at least the following: a method blank, a laboratory control spike ("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the equivalent, where applicable. It should be noted that: • Laboratory fortified blanks are equivalent to LCSs. • Laboratory reagent blanks are equivalent to method blanks. • Post digestion spikes are equivalent to MSs. • Post digestion spike duplicates are equivalent to MSDs. • For method E900.1, used to determine gross alpha, a sample duplicate was used instead ofaMSD. 7 The qualifiers, and the corresponding explanations reported in the QA/QC Summary Reports for any of the check samples for any of the analytical methods, were reviewed by the QA Manager. The QAP Section 8.1.2 requires that a MS/MSD pair be analyzed with each analytical batch. The QAP does not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the MS/MSD pair be prepared on EFRI samples only. Acceptance limits for MS/MSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the QAP requirement to analyze a MS/MSD pair with each analytical batch was met. While the QAP does not require it, the recoveries were reviewed for compliance with each laboratory's established acceptance limits. The QAP does not require this level of review and the results of this review are provided for information only. The information from the Laboratory QA/QC Summary Reports indicates that the MS/MSD recoveries and the associated RPDs for the seeps and springs samples were within acceptable laboratory limits except as noted in Tab E. The MS/MSD recoveries that were outside the laboratory established acceptance limits do not affect the quality or usability of the data, because the recoveries and RPDs above or below the acceptance limits are indicative of matrix interference most likely caused by other constituents in the samples. Matrix interferences are applicable to the individual sample results only. The requirement in the QAPs to analyze a MS/MSD pair with each analytical batch was met and as such the data are compliant with the QAP. The QAP specifies that surrogate compounds shall be employed for all organic analyses, but the QAP does not specify acceptance limits for surrogate recoveries. The analytical data associated with the routine quarterly sampling met the requirement specified in the QAP. The information from the Laboratory QA/QC Summary Reports indicates that the surrogate recoveries for the seeps and springs samples were within acceptable laboratory limits for all surrogate compounds. The QAP Section 8.1.2 requires that each analytical batch shall be accompanied by a reagent blank. Contamination detected in analysis of reagent blanks/method blanks will be used to evaluate any analytical laboratory contamination of environmental samples. The QAP specified process for evaluation of reagent/method blanks states that nonconformance will exist when blanks are within an order of magnitude of the sample results. The information from the Laboratory QA/QC Summary Reports indicates that the reagent (method) blanks for the seeps and springs samples were non-detect and were therefore within the acceptance criteria specified in the QAP. Laboratory duplicates are completed by the analytical laboratories as required by the analytical method specifications. Acceptance limits for laboratory duplicates are set by the laboratories. The QAP does not require the completion of laboratory duplicates or the completion of a QA assessment of them. EFRI reviews the QC data provided by the laboratories for completeness and to assess the overall quality of the data provided. Laboratory duplicate results are provided in Tab D. 5.0 EVALUATION OF ANALYTICAL DATA 8 As previously stated, the samples were analyzed for the groundwater compliance parameters found on Table 2 of the Permit. In addition to these laboratory parameters, the pH, temperature, conductivity, (and although not required, redox and turbidity) were measured and recorded in the field. 5.1 Evaluation of Analytical Results The results of the March and June sampling events shows no evidence of Mill influence in the water produced by the seeps and springs sampled. The lack of Mill influence on seeps and springs is indicated by the fact that the parameters detected are within the ranges of concentrations for the on-site monitoring wells and for available historic data for the seeps and springs themselves. For those detected analytes, concentrations are shown in Tables 2A, 2B, 2C, and 2D. The data are compared to available historic data for each seep and spring as well as to on-site monitoring well data. Specific discussions about each seep or spring are included below. 5.1.1 Ruin Spring No VOCs or radiologies were detected. Metals and major ions were the only analytes detected. The metals detections were minimal with only molybdenum, selenium and uranium having positive detections. A comparison of the 2009 through 2018 data to the 2019 data shows that the concentrations of most detected analytes remained approximately the same with only minor changes within the limits of normal analytical deviation. The reported values for calcium, fluoride, magnesium, nitrate, and molybdenum, increased from the 2018 sample results, but they are below the upper range of historic background values (where available) for the on-site monitoring wells. The differences are not significant and are most likely due to normal fluctuations due to flow rates or seasonal variations due to annual precipitation. Overall, the data reported for Ruin Spring are typical for a surface water sample with no indication of Mill influence. 5.1.2 Cottonwood Spring No VOCs or radiologies were detected. Metals and major ions were the only analytes detected. The metals detections were minimal with only uranium having a positive detection. A comparison of the 2009 through 2018 data to the 2019 data shows that the concentrations of most detected analytes remained approximately the same with only minor changes within the limits of normal analytical deviation. The reported values for bicarbonate, calcium, magnesium, potassium, and sodium increased from the 2018 sample results, but they are below the upper range of historic background values (where available) for the on-site monitoring wells. The differences are not significant and are most likely due to normal fluctuations due to flow rates or seasonal variations due to annual precipitation. Overall, the data reported for Cottonwood Spring are typical for a surface water sample with no indication of Mill influence. 5.1.3 Westwater Seep No radiologies or VOCs were detected. Metals and major ions were detected. The metals detections were minimal with only manganese, and uranium having positive detections. A comparison of the historic data to the 2019 data shows that the concentrations of most detected 9 analytes remained approximately the same with only minor changes within the limits of normal analytical deviation. The reported values for bicarbonate, chloride, potassium, and manganese increased from the 2018 sample results, but they are below the upper range of historic background values (where available) for the on-site monitoring wells. The differences are not significant and are most likely due to normal fluctuations due to flow rates or seasonal variations due to annual precipitation. Overall, the data reported for Westwater Seep are typical for a surface water sample with no indication of Mill influence. 5.1.4 Entrance Spring Gross Alpha, toluene, metals, and major ions were the only analytes detected. The metals detections were minimal with only arsenic, iron, manganese, molybdenum and uranium having positive detections. A comparison of the 2009 through 2018 data to the 2019 data shows that the concentrations of most detected analytes remained approximately the same with only minor changes within the limits of normal analytical deviation. The reported values for bicarbonate, calcium, chloride, fluoride, magnesium, ammonia, potassium, sodium and total dissolved solids ("TDS") increased from the 2018 sample results. The detected concentrations are below the upper range of historic background values (were available) for the on-site monitoring wells. The differences are not significant and are most likely due to normal fluctuations due to flow rates or seasonal variations due to annual precipitation. In addition, the presence of livestock and livestock feces has likely affected the analytical results. Overall, the data reported for Entrance Spring are typical for a surface water sample with no indication of Mill influence. 6.0 CORRECTIVE ACTION REPORT No corrective action reports are required for the 2019 annual sampling event. 6.1 Assessment of Corrective Actions from Previous Period No corrective action reports were required for the 2018 annual sampling event. 7.0 ELECTRONIC DATA FILES AND FORMAT EFRI has provided to the Director electronic copies of the laboratory results as part of the annual seeps and springs monitoring in Comma Separated Values, from the laboratory. A copy of the transmittal e-mail is included under Tab F. 10 11 8.0 SIGNATURE AND CERTIFICATION This document was prepared by Energy Fuels Resources (USA) Inc. Energy Fuels Resources (USA) Inc. By: Scott A. Bakken Senior Director Regulatory Affairs 12 Certification I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and c'omplete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. ~b~~ ..... Scott A. Bakken Senior Director, Regulatory Affairs Energy Fuels Resources (USA) Inc. 13 Tables Table 1: Summary of Seeps and Springs Sampling Work Order - Location Sample Date No.lLab Set ID Dare of Lab Report Cottonwood Spring 6/11/2019 AWAL = 1906343 AWAL = 7/05/2019 GEL= 481772 GEL= 7/10/2019 Entrance Seep 6/11/2019 AWAL = 1906343 AWAL = 7/05/2019 GEL= 481772 GEL= 7/10/2019 Back Spring (Duplicate of 6/11/2019 AW AL= 1906343 AWAL = 7/05/2019 Ruin Spring) GEL= 481772 GEL= 7/10/2019 Ruin Spring 6/11/2019 AW AL= 1906343 AW AL= 7/05/2019 GEL= 481772 GEL= 7/10/2019 Corral Spring Not Sampled -Dry Not Sampled -Dry Not Sampled -Dry Corral Canyon Seep Not Sampled -Dry Not Sampled-Dry Not Sampled-Dry Westwater Seep 3/27/2019 AWAL= 1903737 AWAL = 04/11/2019 GEL =475027 GEL = 04/26/2019 Notes: Multiple dates shown for a single laboratory depict resubmission dates for the data. Resubmissions were required to correct reporting errors. When multiple dates are shown for a single laboratory, the final submission date is shown in italics. Table 2A Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -. Ruin Spring . --. ---. : Range of Average 2011 2011 2018 Historic Avg2003 Constituent 2009 2010 May July 2012 2013 2014 2015 2016 2017 2019 Values for 20042 : Monitoring Wells 1 * -.. ··---.. --.. - Major Ions (mg/I) . Carbonate <l <l <l l <1 <l <l <1 <1 <l <l <l " --- Bicarbonate 233 254 241 239 237 208 204 200 193 208 202 202 ~ : -- Calcium 151 136 145 148 147 149 150 162 138 145 158 165 -- Chloride 28 23 25 44 28 26.3 27.1 27.4 24.4 27.4 29.9 23.9 ND-213 27 Fluoride 0.5 0.53 0.45 0.5 0.52 0.538 <1 0.445 0.541 0.5 0.414 0.505 ND-1.3 0.6 Magnesium 32.3 29.7 30.6 31.1 31.9 32.1 35.4 31.8 31.1 30.2 33.9 45.6 --- Nitrogen-Ammonia 0.09 <0.05 ND <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 --:;_ I Nitrogen-Nitrate 1.4 1.7 1.7 1.6 l.6 1.56 1.54 1.31 1.64 1.55 1.35 1.56 ---. Potassium 3.3 3.07 3.2 3.3 3.5 3.46 3.24 3.14 3.18 3.07 3.58 3.31 ··-· -.. . --· Sodium 104 93.4 110 111 115 118 119 126 105 113 128 128 --- Sulfate 528 447 486 484 464 553 553 528 490 476 547 474 ND-3455 521 TDS 1010 903 942 905 1000 952 984 1000 916 972 1000 900 1019-5548 1053 Metals (ug/1) Arsenic <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 --;- Beryllium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -.. Cadmium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND -4.78 0.01 Chromium <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 -- Cobalt <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ' ---. Copper <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 --- Iron <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 <30 ND-7942 25 Lead <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ---- Manganese <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ND-34,550 5 Mercury <0.5 <0.5 <0.5 <0.S <0.S <0.5 <0.S <0.5 <0.S <0.S <0.5 <0.S ---- Molybdenum 17 17 16 17 16 16.1 16.0 18.3 17.8 17.2 18 20.2 --- Nickel <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 ND-61 0.05 Table 2A Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells .. Ruin Spring . ---'" ---• -I Range of -I I Average Constituent 2009 2010 2011 2011 2012 2013 2014 2015 2016 2017 2018 2019 Historic Avg 2003 May July Values for 20042 . I Monitoring Wells 1 * ·-' Selenium 12.2 10 11.8 10.2 10.8 10.2 12 10 10 10.5 12.2 10.8 ND-106.5 12.1 Silver <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 -· - Thallium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 --- Tin <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 -' - Uranium 9.11 8.47 9.35 8.63 8.68 9.12 9.61 9.03 8.38 8.49 9.35 9.02 ND-59.8 IO Vanadium <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 --- Zinc <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 --· -- Radiologies (pCi/1) Gross Alpha <0.2 <0.2 <-0.3 <-0.05 <-0.09 <1.0 <l <1.0 <1.0 <1.0 <1.57 <1.0 ND-36 0.28 voes (ug/L) Acetone <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 -- Benzene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 <1.0 <l.0 <l.0 --- Carbon tetrachloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <LO <1.0 <1.0 <l.0 <1.0 --- Chloroform <1.0 <l.0 <1.0 <1.0 <LO <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --.. - Chloromethane <1.0 <1.0 <LO <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 --- MEK <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 --- Methylene Chloride <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 --: '•:-·- Naphthalene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ---- Tetrahydrofuran <1.0 <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 --· Toluene <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 <1.0 -- Xylenes <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- 1 From Figure 3, Table 10 and Appendix B of the Revised Addendum, Background Groundwater Quality Report: New Wells.for Denison Mines (USA) Corp 's White Mesa Mill Site, San Juan County. Utah. April 30, 2008, prepared by INTERA, Inc. and Table 16 and Appendix D of the Revised Background Groundwater Quality Report: Existing Wells fc,r Denison Mines (USA) Corp. 's White Mesa Uranium Mill Site, San Juan County, Utah, October 2007, prepared by INTERA, Inc. 2 From Figure 9 of the Revised Addendum, Evaluation of Available Pre-Operational and Regional Background Data, Background Groundwater Quality Report: Existing Wells.for Denison Mines (USA) Corp. 's White Mesa Mill Site. San Juan Couinty, Utah, November 16, 2007, prepared by INTERA. Inc. . *Range of average historic values for On-Site Monitoring Wells as reported on April 30, 2008 (MW-I, MW-2, MW-3, MW-3A, MW-4, MW-5, MW-I I, MW-12, MW-14, MW-15, MW-17. MW-I 8, MW- 19, MW-20, MW-22, MW-23, MW-24, MW-25, MW-26, MW-27, MW-28, MW-29, MW-30, MW-31 and MW-32)2 Table 2B Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -Cottonwood Spring .,. . ' ,. . --Range of . ' . -Average 2011 2011 Historic Avg 1977 Constituent 2009 2010 May July 2012 2013 2014 2015 2016 2017 2018 2019 Values for 1982 I Monitoring I Wells1* . " . > Major Ions (mg/I) I Carbonate <1 <1 <1 6 <1 <1 <1 <1 <l <l <1 <1 ---,1 -.... . -Bicarbonate 316 340 330 316 326 280 251 271 256 280 283 286 --- Calcium 90.3 92.2 95.4 94.2 101 87.9 99.7 Ill 102 99.6 109 122 -- Chloride 124 112 113 134 149 118 128 133 138 129 153 138 ND -213 31 Fluoride 0.4 0.38 0.34 0.38 0.38 0.417 <l 0.318 0.466 0.344 0.282 0.249 ND -1.3 0.8 Magnesium 25 24.8 25 .2 25 .2 27.7 23.6 29.0 27.5 29.5 27.1 30.2 35.3 -., --.. Nitrogen-. .. <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 0.0512 <0.05 <0.05 ' <0.05 <0.05 . -.. Ammonia I Nitrogen-Nitrate 0.1 <0.1 0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 0.124 0.108 <0.1 , -.--' Potassium 5.7 5.77 6 5.9 6.2 5.53 6.18 5.91 6.11 5.72 6.35 6.78 -i -- Sodium 205 214 229 227 247 217 227 251 221 213 234 268 -- Sulfate 383 389 394 389 256 403 417 442 443 409 428 423 ND-3455 230 TDS 1010 900 1030 978 1040 996 968 1020 1070 1080 1080 1010 1019-5548 811 . .., Metals (ug/1) Arsenic <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 -· -· Beryllium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -.. Cadmium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND-4.78 ... . Chromium <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 --- Cobalt <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 --· -- Copper <10 <10 <10 <10 <10 <10 <10 ~ <10 <10 <10 <10 <10 --- Iron <30 <30 53 <30 <30 <30 <30 <30 <30 <30 <30 <30 ND-7942 150 Lead <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -.. Manganese <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ND-34,550 580 Mercury <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ~ --- Molybdenum <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ---- Nickel <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 ND-61 - Selenium <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5 <5 <5 <5 <5 ND -106.5 - Table 2B Detected Constituents and Comparison to Historic Values and Mill Site Monitoring Wells -. Cottonwood Spring --. -------. --I I I Range of I Average Constituent 2009 2010 2011 2011 2012 2013 2014 2015 2016 2017 2018 2019 Historic Avg 1977 May July Values for 1982 1 I Monitoring I Wells1* .. ·- Silver <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 -.;_ '· . -Thallium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <0.5 <0.5 <0.5 --- Tin <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 -- Uranium 8.42 8.24 7.87 8.68 8.17 8.95 9.62 9.12 8.84 9.17 10.3 10.1 ND-59.8 -- Vanadium <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 ---- Zinc <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ---.. - Radiologies (pCi/1) Gross Alpha <0.2 <0.2 <0.1 <-0.1 <-0.2 <1.0 <1.0 <1.0 <1.0 <1.0 <LO <1.0 ND-36 7.2 -voes (ug/L) Acetone <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 -· - Benzene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- Carbon <LO <1.0 <1.0 <LO <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 tetrachloride --- Chloroform <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ' ' --.. -- Chloromethane <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ' -.. . -. MEK <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 i -.. , . Methylene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Chloride --,-- Naphthalene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <LO <1.0 <1.0 <1.0 <1.0 <1.0 . --- Tetrahydrofuran <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ---- Toluene <1.0 <1.0 <LO <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <LO <1.0 <LO I I .. ! -.. Xylenes <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ' <LO <1.0 <1.0 <1.0 <1.0 <1.0 .. I -: 1 From Figure 3, Table IO and Appendix B of the Revised Addendum, Background Groundwater Quality Report: New Wells for Denison Mines (USA ) Corp's White Mesa Mill Site. San Juan County, Utah , April 30, 2008. prepared by INTERA, Inc. and Table I 6 and Appendix D of the Revised Backxround Groundwater Quality Report: Existinx Wells f or Denison Mines ( USA) Corp. 's White Mesa Uranium Mill Site. San Juan County, Utah, October 2007, prepared by INTERA, Inc. *Range of average historic values for On-Site Monitoring Wells as reported on April 30, 2008 (MW-I , MW-2, MW-3, MW-3A. MW-4, MW-5, MW-I I, MW-1 2, MW-14, MW-15, MW-17, MW- 18, MW-19, MW-20, MW-22, MW-23. MW-24. MW-25, MW-26. MW-27, MW-28, MW-29, MW-30, MW-3 land MW-32) I Table 2C Detected Constituents and Com_J)_arison to Historic Values and Mill Site Monitoring_ Wells .. Westwater S~p . -. -. ----·----Range of · i I I I Average Constituent 2009 2010 2011 May 2011 July 2012 2013 2014 2015 2016 2017 2018 -2019 Historic Values for I --~ • 1-~ --., Monitoring Wells1 * . ' ---.. ---MajQr Ions (m2'1) --. ------ Carbonate <l <I <l <1 <I <I <l <I - Bicarbonate 465 450 371 359 399 369 444 450 --Calcium 191 179 247 150 176 125 204 185 - Chloride 41 40 21 32.6 38.0 27.5 36.2 41.6 ND -213 Fluoride 0.7 0.6 0.54 0.424 0.618 0.574 0.659 0.505 ND-1.3 Magnesium 45.9 44.7 34.7 Not Sampled Not Sampled Not Sampled Not Sampled 34 47.3 31.7 56.6 43.7 - Nitrogen-Ammonia <0.05 0.5 0.06 Dry Dry Dry Dry 0.123 <0.05 <0.05 0.0832 <0.05 -- Nitrogen-Nitrate 0.8 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 - Potassium 1.19 6.57 3.9 1.98 2.32 2.33 2.94 3.99 - Sodium 196 160 112 139 185 133 218 152 - Sulfate 646 607 354 392 573 318 580 436 ND-3455 TDS 1370 1270 853 896 1060 820 1220 1110 1019 -5548 -Metals (.ue./1) - Arsenic <5 <5 12.3 <5.0 <5.0 <5.0 <5.0 <5.0 .- Beryllium <0.5 <0.5 0.91 <0.5 <0.5 <0.5 <0.5 <0.5 - Cadmium <0.5 <0.5 0.9 <0.5 <0.5 <0.5 <0.5 <0.5 ND-4.78 Chromium <25 <25 <25 <25 <25 <25 <25 <25 --Cobalt <10 <IO <IO <IO <10 <10 <10 <10 ---- Copper <10 <10 16 <10 <10 <10 <IO <10 - Iron 89 56 4540 <30 40.1 181 575 1.20 ND-7942 Lead <1.0 <1.0 41.4 <1.0 <1.0 <1.0 <1.0 <1.0 - Manganese 37 87 268 171 55.5 144 312 528 ND-34,550 Mercury <0.5 <0.5 <0.5 Not Sampled Not Sampled Not Sampled Not Sampled <0.5 <0.5 <0.5 <0.5 <0.5 Dry Dry Dry Dry - Molybdenum 29 29 <10 <10 <10 <10 <10 <10 - Nickel <20 <20 29 <20 <20 <20 <20 <20 ND-61 Selenium <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 ND-106.5 Silver <10 <IO <IO <10 <10 <10 <10 <10 --- Thallium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -- Tin <100 <100 <100 <100 <100 <100 <100 <100 -- Uranium 15.1 46.6 6.64 2.1 19.0 5.17 13.2 4.92 NP-59.8 Vanadium <15 <15 34 <15 <15 <15 <15 <15 - Zinc <10 <10 28 <10 <10 <10 <10 <10 . -- Table 2C Detected Constituents and Comparison to Historic Values and Mill Site Monitoring_ Wells -·-------. ---Westwater Seep --Range of Average Constituent 2009 2010 2011 May 2011 July 2012 2013 2014 2015 2016 2017 2018 2019 Historic Values for Monitoring ' Wells1 * ---r~ --,J': ------.. ' Radiolc Irie$ (1>Ci/J) ----·· ----- Gross Alpha < -0.1 <0.3 0.5 Not Sampled Not Sampled Not Sampled Not Sampled <1.0 <1.0 <1.0 <1.0 <l.0 ND-36 Dry Dry Dry Dry VOCS{ufdL) ---· ---Acetone <20 <20 <20 <20 <20 23.1 <20 <20 ----- Benzene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Carbon tetrachloride <LO <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Chloroform <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --Chloromethane <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - MEK <20 <20 <20 Not Sampled Not Sampled Not Sampled Not Sampled <20 <20 <20 <20 <20 Dry Dry Dry Dry -- -Methylene Chloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 - Naphthalene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 -, Tetrahydrofuran <1.0 <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Toluene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Xylenes <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 - From Figure 3, Table IO and Appendix B of the Revised Addendum. Background Groundwater Qua/ii)' Report: New Wells for Denison Mines (USA) Corp 's Whire Mesa Mill Site, San Juan Counry, Utah, April 30, 2008, prepared by INT ERA, Inc. and Table 16 and Appendix D of the Revised Background Groundwater Quality Report: Existing Wells for Denison Mines ( USA) Corp. 's White Mesa Uranium Mill Site, San Juan County, Utah, October 2007, prepared by INTERA, Inc. *Range of average historic values for On-Site Monitoring Wells as reported on April 30, 2008 (MW-1, MW-2, MW-3, MW-3A, MW-4, MW-5, MW-I I, MW-I 2, MW-14, MW-15, MW-17, MW-18, MW-19, MW-20, MW-22, MW-23, MW-24, MW-25, MW-26, MW-27, MW-28, MW-29, MW-30, MW-31 and MW-32) Table 20 Detected Constituents and Comparison to Historic Values and Mill Site Monitorin,g Wells Entrance Spring -. ' ---·. ----. ---. -.. ----.. -I Range of Average Constituent 2009 2010 2011 May 2011 July 2012 2013 2014 2015 2016 2017 2018 2019 Historic Values for Monitoring I Wells1* cl --... -. --- Major Ions (mg/I) . -- Carbonate <1 <1 <1 7 <l <l <l <l <l <I <I <I I .I ; -l .... "'-_:J \ _, Bicarbonate 292 332 270 299 298 292 247 324 340 402 236 480 -• -~:ii~ \ Calcium 90.8 96.5 88.8 96.6 105 121 103 131 131 129 116 155 Chloride 60 63 49 64 78 139 76.8 75.6 75 84.6 75.9 104 ND-213 Fluoride 0.7 0.73 0.58 0.58 0.64 0.71 <1 0.606 0.668 0.615 0.454 0.912 ND -1.3 Magnesium 26.6 28.9 26.4 28.4 32.7 43 34.9 33.3 38.6 36.4 42.4 48.0 - Nitrogen-Ammonia 0.28 <0.05 <0.05 0.32 <0.05 <0.05 <0.05 0.202 0.0962 0.247 0.102 0.168 --:- Nitrogen-Nitrate 1.4 1 1.4 0.5 2.8 2.06 3.65 <0.1 0.403 <1 2.34 <1 - Potassium 2.4 2.74 2.6 2.9 2 3.83 1.56 1.62 <1.0 3.88 3.64 4.66 - Sodium 61.4 62.7 62.5 68.6 77.4 127 78.9 93.1 90.8 90.3 96 126 - Sulfate 178 179 166 171 171 394 219 210 245 187 243 160 ND-3455 TDS 605 661 571 582 660 828 688 680 828 752 820 892 1019 -5548 -Metals (ug/.1) - Arsenic <5 <5 <5 <5 <5 <5 <5 5.02 <5 9.16 <5 8.94 " -- Beryllium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -- Cadmium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND -4.78 Chromium <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 <25 - Cobalt <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 .. - Coover <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 .. Iron <30 <30 37 55 34 162 37.2 295 94.4 371 <30 453 ND-7942 Lead <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -· Manganese 54 11 47 84 <10 259 16.1 367 210 913 405 587 ND-34,550 Mercury <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 -- Molvbdenum <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 14.30 -- Nickel <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 ND-61 Selenium 12.1 9.2 13.1 5.5 13.2 11.2 15.9 <5 <5 <5 15.3 <5 ND -106.5 Silver <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 - Thallium <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 - Tin <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 - Uranium 15.2 17.8 18.8 15.3 21.1 38.8 23.2 36 22.0 14.6 27.6 70.1 ND-59.8 Vanadium <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 <15 -., Zinc <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 - Table 20 Detected Constituents and Comparison to Historic Values and Mill Site Monitori ng Wells -.. --Entrance Sptiog .. -----. -'. - ; I Range of Average Historic V aloes Constituent 2009 2010 2011 May 2011 July 2012 2013 2014 2015 2016 2017 2018 2019 for Monitoring -Wells1* I ------·-. --- --Radiologies (pCi/1) Gross Alpha 0.9 <0.5 I 1.5 1.6 0.5 2.3 <I 3.05 <I 2.53 <1 2.63 ND-36 VOCS{ug/L) ' Acetone <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 -- Benzene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- Carbon tetrachloride <1.0 <l.0 <l.0 <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 -- Chloroform <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 --. Chloromethane <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 ---- MEK <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 <20 - Methylene Chloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 <1.0 - Naphthalene <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 - Tetrahydrofuran <1.0 <l.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <l.0 <1.0 <1.0 <l.0 - Toluene <1.0 <1.0 <1.0 <1.0 <1.0 <LO 1.32 <1.0 <1.0 13.1 <1.0 5.59 -- Xvlenes <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 -- 1 From Figure 3, Table l O and Appendix B of the Revised Addendum, Background Groundwater Quality Report: New Wells for Denison Mines ( USA) Corp 's White Mesa Mill Site, San Juan County, Utah, April 30, 2008, prepared by INTERA, Inc. and Table 16 and Appendix D of the Revised Background Groundwater Quality Report: Existing Wells for Denison Mines (USA) Corp. 's White Mesa Uranium Mill Site, San Juan County, Utah, October 2007, prepared by INTERA, Inc. *Range of average historic values for On-Site Monitoring Wells as reported on April 30, 2008 (MW-I, MW-2, MW-3, MW-3A, MW-4, MW-5, MW-I 1, MW-12, MW-14, MW-15, MW- 17, MW-18, MW-19, MW-20, MW-22, MW-23, MW-24, MW-25, MW-26, MW-27, MW-28, MW-29, MW-30, MW-31 and MW-32) - ': - . ' I INDEX OF TABS Tab A Seeps and Springs Field Data Sheets and Photographic Documentation Tab B Field Parameter Measurement Data Tab C Survey Data and Contour Map Tab D Analytical Laboratory Data Tab E Quality Assurance and Data Validation Tables E-1 Holding Time Evaluation E-2 Laboratory Receipt Temperature Check E-3 Analytical Method Check E-4 Reporting Limit Evaluation E-5 Trip Blank Evaluation E-6 QNQC Evaluation for Sample Duplicates E-7 Radiologic Counting Error E-8 Laboratory Matrix QC Evaluation Tab F CSV Transmittal Tab A Seeps and Springs Field Data Sheets and Photographic Documentation Field Data Record-Seeps and Springs Sampling Seep or Spring Location: .....:C:-...o ..... +"'-· ii"""'< ..... )tl ........... L,>, ..... ).._.Q.,_O .... d __ .s"'""pr-,_._1 Q..,_:J=t---------- Date For Initial Sampling Visit: C;,/ 11 / :l O I q Time:_~O_'i.......:S ...... a ______ _ Sample Collected: 111 Yes o No Date For Second Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes o No Date For Third Sampling Visit: _______ Time: .. ---------- Sample Collected: o Yes D No Sampling Personnel: "'-oaer Holl ;d~ , Deea L~~aa , Deoo W,odecs OQ Weather Conditions at Time of Sampling: __ :;i ..... ,_:1,o ..... a ..... ,..,~------------ Estimated Seep or Spring Flow Rate: • 5 0 0 6-P M --------'~__....__ _______ _ Field Parameter Measurements: -pH -Temperature (°C) _---'-t 5.._.,._q.._7 __________ _ -Conductivity µMHOC/cm --i~1-Q~(--------- -Turbidity (NfU) (if measured). ________ _ -Redox Potential Eh (mV) (if measured) _J..t ..... -Z ........... O ___ _ Analytical P.arameters/Sample Collection Method: Iii Yes oNo oYes mNo D ijll Metals fiJ Yes oNo Iii Yes oNo D l!l Nutrients Iii Yes ONo oYes lil No 0 ril OtherNon WYes i;:iNo oYes ~No D ~ Radiofo ·cs Gross Alpha l3J Yes oNo Yes oNo D ~ QC Samples Associated with this Location: o Rinsate Blank o Duplicate Duplicate Sample Name: __________ _ D D D D D Notes: Accipea aa ~;±c o..+ D4'io So,mpks '-Dlleckd o,.± 0950 wo..±«:c w)a s c: I eo.c. D D 0 0 Field Data Record-Seeps and Springs Sampllne Seep or Spring Location: "F-n+r~n ce Seep Date For Infdal Sampling Visit: C..,/ 11 / J,O I q Sample Collected: ij1J Yes p No Time: 0 'i> IS Date For Second Sampling Visit: ________ Time: ________ _ Sample Collected: o Yes o No Date For Third Sampllng Visit: _______ Time: _________ _ Sample Collected: D Yes D No Sampling Personnel: ~aaec Non;Jt3 I Dee() L~Wlq./)' Dean H,ndec.soq Weather Condidons at Time of Sampllng:_s~· \A-"--,...-::-j~------------ Esdmated Seep or Spring Flow Rate: wer ! ,)c.. '> llijO o.rd: I f1D \?;.S, b4 l -How FJeld Parameter Measurements: -pH -Temperature (°C) _.........,~~----------- -Conductivity µMHOC/cm _,_, ~-'-"-';z.....,;: ________ _ -Turbidity (NTU) (ifmeasured) __ fo~3', ..... $._ _____ _ -Redox Potential Eh (mV) (if measured) _:5.__.-, ..... z ____ _ Analytical P.arameters/Sample Collection Method: Iii Yes oNo DYes o!1 No D ti!! D D Metals OOYes oNo ~Yes oNo D ~ D D Nutrients Ill Yes oNo oYes ijJ No D lJI D 0 Other Non ~Yes oNo oYes [)I No D ijl D D Radiofo ·cs Gross Alpha [ii Yes DNo ~Yes oNo D 11} D D QC Samples Associated with this Location: o Rinsate Blank o Duplicate Duplicate Sample Name: Field Data Record-Seeps and Springs Sampling Seep or Spring Location: ---:.cB ..... tA.___c.k----""_s. ..... • pr-r_i n ............. ji----------------- Date For Initial Sampling Visit: b / 11 / 2. 0 I q Sample Collected: ~ Yes o No Time: 0 850 Date For Second Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes o No Date For Third Sampling Visit: ________ Time: _________ _ Sample Collected: o Yes o No Sampling Personnel: ~.;..xO.,...tl...._(l .... eC---'~--'o=H,....; l~~~t-1 ..... D...,,.,;;.o.e .... o ........... L...,,~~{""-W)""'Afl:......;-1-D .... e ..... o ..... o-'--lUJ..l,e,d.01'J.e..!.e..Lc ..... s~o,!./.q.!,.__ Weather Conditions at Time of Sampling: ___ s_· ~"'-o .... o ..... jr------------- Estimated Seep or Spring Flow Rate: __ ...._J ...... 0...._--G-,__.f ..... t'\'-+---------- Field Parameter Measurements: -pH -Temperature (°C) __.1._3 ......... e, ..... C:.___ _________ _ -Conductivity µMHOC/~ __._l~ .......... s·:1-+---------- -Turbidity (NTU) (if measured)~D=--------- -Redox Potential Eh (m V) (if measured) _,3 .... 8 ...... 7 ____ _ Analytical Parameters/Sample Collection Method: rsnYes oNo oYes 1!1 No Metals Iii Yes oNo ljl Yes DNo Nutrients Iii Yes oNo OYes l¥l No Other Non ~Yes DNo oYes MNo Radiofo 'cs Gross Alpha [ii Yes oNo Yes oNo QC Samples Associated with this Location: o Rinsate Blank 181 Duplicate ll!I D B:l Iii D D D D Bl Duplicate Sample Name: ___________ _ D D D D D Notes: Ar ri11ea D(\ 5 ,±, a-.± 0$,j () So.mplcs c..olledc:d 0:-± bX{b O Wo.t«: l,,,)Gi."'> C-leCX:::: D D D D Field Data Record-Seeps and Springs Sampli.n.& Seep or Spring Location: -'-'R=-=u..-=;-'-'i\_S--+p_r_; "-:~:::r------------- Date For Initial Sampling Visit: (,.._./ 11 /:J., 0 I q Time: 085D . __,......,.......: _____ _ Sample Collected: ~ Yes o No Date For Second Sampling Visit: Time: --------- Sample Collected: o Yes D No t, Date For Third Sampling Visit: Time: --------- Sample Collected: D Yes o No Sampling Personnel: ---r;_ooer ~on ;J't3 , Deeo L~t11) , Deao ~endec.s.oq ~eather Conditions at Time of Samplin.g: 5 ..... (\"1- Estimated Seep or Spring Flow Rate: ___.}-'-. =O_ ..... (,: ..... P_.9b1___._ __________ _ Field Parameter Measurements: -pH 7, i.iO -Temperature (°C) __ 1~---'''-=<..=~'----------- -Conductivity µMHOC/cm ~l?..~5 -'1 _______ _ -Turbidity (NTU) (if measured) ___ ...___ ___ 9 ___ _ -Redox Potential Eh (mV) (if measured) _3"-&'"""'"'---- Analytical Parameters/Sample Collection Method: voes Iii Yes oNo oYes 111 No ti 0 D D Metals Iii Yes oNo Iii Yes DNo D Ill D D Nutrients 111 Yes oNo oYes ljl No ii 0 D 0 OtherNon ~Yes oNo oYes Iii No ~ D D D Radiolo ·cs Gross Alpha !:ii Yes oNo ~Yes oNo D Ci!I D D QC Samples Associated with this Location: ~ . o Rinsate Blank ,. o Duplicate Duplicate Sample Name: __________ _ Notes: Acd\)ea DQ s;+, d-0 kjo So..mpks (..olleded o± o gso Wo..±ec luci.5 Glel).[. Field Data Record-Seeps and Springs Sampling Seep or Spring Location: LJe~+4)<X.+er S~~p Date For Initial Sampling Visit: 3 /f)..l) /~D I'\ Sample Collected: D Yes !J No Date For Second Sampling Visit: 3 /:;_7 /;2.01'1 Sample Collected: WY es o No Time: 0913 Time: 0 q3Q Date For Third Sampling Visit: _______ Time: ________ _ Sample Collected: o Yes o No SamplingPersonnel: ~MCI""' Uoll i'kj I Do-n L~r1c..n Weather Conditions at Time of Sampling:__,,e,c...l'""'c, ...... v .... J:j .... ~----------- Estimated Seep or Spring Flow Rate: Lou ~I ow . -~~~~------------ Field Parameter Measurements: -pH -Temperature (°C) __.l ...... l ....... 7 ...... 2. _________ _ -Conductivity µMHOC/cm _l ..... '1 ..... ;1..-=5<....._ _______ _ -Turbidity (NTU) (if measured)__.._,.,..:.....,.,_ ______ _ -Redox Potential Eh (mV) (if measured) ,3$S ~ ---- Analytical Parameten/Sample Collection Method: voes MYes DNo oYes Q9 No D L!I Metals ~Yes ONo i;g Yes DNo D Bl Nutrients Bl Yes DNo oYes Bl No D Bl Other Non ~Yes oNo DYes Ii No D ~ Radiolo cs Gross Alpha BJ Yes oNo !JI Yes DNo D IY1 QC Samples Associated with this Location: o Rinsate Blank o Duplicate Duplicate Sample Name: Notes: Arri\lcd on ~i'tc ~+ 09:i.s s .. Mf>lt'.'C, c:olledeJ p;d·ul"(. t..)<t:<:, + Gt \C C,l'I • Lc:£:1 s.; ..... o.+ O'f 'iO . D D D D D D D D D D "'+ D9.3D . ( Field Data Record~Seeps and Springs Sampling Seep or Spring Location: C. oro-. \ {,C\O ~on Seep G. \ Date For Initial Sampling Visit: 3/2-,0 /2-[) !q Time: __ Q~9_L.j..._fo ____ _ Sample Collected: o Yes ~ No G.::2.._ Date For Second Sampling Visit: b / 11 / 2,() IC\ Time: l.?...3 i Sample Collected: o Yes 1iJ No G(3 Date For Third Sampling Visit: g, / r I ~O 19 Time: }M :S Sample Collected: o Yes ~ No Sampling Personnel: Weather Conditions at Time of Sampling: ---------------- Estimated Seep or Spring Flow Rate: ----------------- Field Parameter Measurements: -pH -Temperature (°C) ______________ _ -Conductivity µMHOC/cm ___________ _ -Turbidity (NTU) (if measured) _________ _ -Redox Potential Eh (mV) (if measured) ______ _ Analytical Parameters/Sample Collection Method: Parameter , Sample Taken Filtered II ,SaJlipling M"lhojJ, I Direct 11 Peristaltic 'Ladle Other ' 11 ,, Pump ( describe in anotes section) voes oYes oNo o Yes ONo D D 0 D Metals oYes oNo oYes oNo 0 D 0 D Nutrients oYes oNo oYes oNo D 0 0 0 Other Non oYes oNo oYes oNo D D D D Radiologies Gross Alpha oYes oNo oYes oNo D 0 0 0 QC Samples Associated with this Location: o Rinsate Blank o Duplicate Duplicate Sample Name: __________ _ Notes: Gr-\ pi(. 1,.)~S,, ±<)\ken ,j-08 .SY' Field Data Record-Seeps and Springs Sampling Seep or Spring Location: _ .. C~o~CC~P..~/ ~.S~p~r-~Qg--1.--------------- Q l Date For Initial Sampling Visit: 3,/ :LOI AA l~ Sample CoJlected: D Yes ~ No Qd... Date For Second Sampling Visit: C, /t l /2.019 Sample Collected: D Yes ~ No Q3 Date For Third Sampling Visit: g/ 7/:)..01q Sample Collected: o Yes lWNo Sampling Personnel: Time: 0·933 Time: I Z 1 t-/ Time: t;LD1 Weather Conditions at Time of Sampling: ______________ _ Estimated Seep or Spring Flow Rate: ----------------- Field Parameter Measurements: -pH -Temperature (°C) _____________ _ -Conductivity µMHOC/cm ----------- -Turbidity (NTU) (if measured) -----------Redo x Potential Eh (m V) (if measured) ______ _ Analytical Parameters/Sample Collection Method: voes DYes DNo oYes DNo D D Metals oYes oNo oYes oNo D D Nutrients DYes DNo oYes DNo D D Other Non oYes DNo oYes oNo D D Radiolo ·cs Gross Alpha DYes DNo oYes DNo D D QC Samples Associated with this Location: o Rinsate Blank o Duplicate Duplicate Sample Name: D D D D D Notes: QL{ ' +"' Uen °'-t o ~~O . ~ ~ ~a&Jrd· f?ll:.';:;, S cp r'"j D D D D D TabB Field Parameter Measurement Data Field parameter . Date Location Saml)led pH C_onductivity Turbidity Redox Temperature Cottonwood Spring 6/11/2019 7.09 1701 0 470 15.97 Entrance Seep 6/11/2019 7.09 1425 63.8 517 14.02 Back Spring (Duplicate of Ruin Spring) 6/11/2019 7.40 1254 0 387 13.66 Ruin Spring 6/11/2019 7.40 1254 0 387 13.66 Westwater Seep 3/27/2019 7.14 1628 11.7 355 11.72 TabC Survey Data and Contour Map Seeps and Springs Survey Locations Mid-December 2009 Survey Location Latitude (N) Longitude (W) Elevation FROG POND 37°33'03.5358" 109°29'04.9552" 5589.56 CORRAL CANYON 37°33'07.1392" 109°29'12.3907" 5623.97 ENTRANCE SPRING 37°32'01.6487" 109°29'33.7005" 5559.71 CORRAL SPRINGS 37°29'37.9192" 109°29'35.8201" 5383.35 RUIN SPRING 37°30'06.0448" 109°31'23.4300" 5380.03 COTTONWOOD 37°3 l '21.7002" 109°32'14.7923" 5234.33 WESTWATER 37°31'58.5020" 109°31 '25.7345" 5468.23 Verification Survey July 2010 RUIN SPRING 37°30'06.0456" 109°31 '23.4181" 5380.01 COTTONWOOD 37°3 l '21.6987" 109°32'14.7927" 5234.27 WESTWATER 37°31'58.5013" 109°31 '25.7357" 5468.32 @ estimated dry area TW4-42 temporary perched monitoring well ¢ 5528 installed April, 2019 showing elevation in feet amsl MW-38 perched monitoring well "9-5462 installed February, 2018 showing elevation in feet amsl TW4-40 temporary perched monitoring well -+,5527 installed February, 2018 showing elevation in feet amsl M:';5 503 perched monitoring well showing elevation in feet amsl TW4-12 . . 0 5571 temporary perched momtonng well showing elevation in feet amsl TWN-7 d . . . <>5567 temporary perche nitrate momtonng well showing elevation in feet amsl PIEZ-1 perched piezometer showing -1 5589 elevation in feet amsl RUIN SPRING o 5380 seep or spring showing elevation in feet amsl NOTES: MW-4, MW-26, TW4-1, TW4-2, TW4-4, TW4-11, TW4-19, TW4-20, TW4-21, TW4-37, TW4-39, TW4-40 and TW4-41 are chloroform pumping wells; TW4-2.2, TW4-24, TW4-25 and TWN-2 are nitrate pumpin.9. wells; TW4-11 water level is below the base of the Burro Canyon Formation HYDRO GEO CHEM, INC. KRIGED 3rd QUARTER, 2019 WATER LEVELS {DR PIEZOMETERS NOT INCLUDED) WHITE MESA SITE APPROVED DATE REFERENCE H:/718000/nov19/WL/Uwl0919nodr.srf FIGURE C-1 @ TW4-42 ¢5528 MW-38 -<?-5462 estimated dry area temporary perched monitoring well installed April, 2019 showing elevation in feet amsl perched monitoring well installed February, 2018 showing elevation in feet amsl TW-440 temporary perched monitoring well -+-5527 installed February, 2018 showing elevation in feet amsl M:55 503 perched monitoring well showing elevation in feet amsl TW4-12 0 5571 temporary perched monitoring well showing elevation in feet amsl TWN-7 t h d ·1 . . .A.5567 emporary perc e m rate monitoring V well showing elevation in feet amsl PIEZ-1 perched piezometer showing g 5589 elevation in feet amsl RUIN SPRING & 5380 seep or spring showing elevation in feet amsl NOTES: MW-4, MW-26, TW4-1 , TW4-2, lW4-4, TW4-11, TW4-19, TW4-20, lW4-21, TW4-37, TW4-39, TW4-40 and TW4-41 are chloroform pumping wells; TW4-22, TW4-24, TW4-25 and lWN-2 are nitrate p_umpin!I_ wells; lW4-11 water level is below the base of the Burro Canyon Formation HYDRO GEO CHEM,INC. KRIGED 3rd QUARTER, 2019 WATER LEVELS WHITE MESA SITE APPROVED DATE REfERENCE H:/718000/nov19/WUUwl0919dr.srf FIGURE C-2 TabD Analytical Laboratory Data INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps and Springs 2019 Lab Sample ID: 1903737-001 Client Sample ID: Westwater Seep ANALYTICAL LABORATORIES Collection Date: 3/27/2019 930h Received Date: 3/29/2019 1000h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qua) ;;alt Lake City, UT 84119 Arsenic mg/L 4/5/2019 I 023h 4/8/2019 1225h £200.8 0.00500 < 0.00500 Beryllium mg/L 4/5/2019 I 023h 4/9/2019 1737h £200.8 0.000500 < 0.000500 Cadmium mg/L 4/5/2019 1023h 4/8/2019 1225h £200.8 0.000500 < 0.000500 Calcium mg/L 4/5/2019 1023h 4/10/2019 1316h £200.7 10.0 185 Phone:(801)263-8686 Chromium mg/L 4/5/2019 1023h 4/8/2019 1225h £200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 4/5/2019 1023h 4/8/2019 1225h £200.8 0.0100 < 0.0100 Fax: (80 I) 263-8687 Copper mg/L 4/5/2019 I 023h 4/8/2019 1225h £200.8 0.0100 < 0.0100 !-mail: awal@awal-labs.com Iron mg/L 4/5/2019 1023h 4/10/2019 1523h £200.8 0.100 1.20 Lead mg/L 4/5/2019 I 023h 4/9/2019 1737h £200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 4/5/2019 1023h 4/10/2019 1316h £200.7 10.0 43.7 Manganese mg/L 4/5/2019 1023h 4/8/2019 1225h £200.8 0.0100 0.528 B Mercury mg/L 4/4/2019 1830h 4/10/2019 830h £245.1 0.000500 < 0.000500 Kyle F. Gross Molybdenum mg/L 4/5/2019 1023h 4/8/2019 1225h £200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 4/5/2019 I 023h 4/9/2019 1728h £200.8 0.0200 < 0.0200 Potassium mg/L 4/5/2019 1023h 4/10/2019 1329h £200.7 1.00 3.99 Jose Rocha Selenium mg/L 4/5/2019 1023h 4/8/2019 1225h £200.8 0.00500 < 0.00500 QA Officer Silver mg/L 4/5/2019 I 023h 4/9/2019 1728h £200.8 0.0100 < 0.0100 Sodium mg/L 4/5/2019 I 023h 4/10/2019 1316h £200.7 10.0 152 Thallium mg/L 4/5/2019 1023h 4/9/2019 1737h £200.8 0.000500 < 0.000500 Tin mg/L 4/5/2019 I 023h 4/8/2019 1225h £200.8 0.100 < 0.100 Uranium mg/L 4/5/2019 1023h 4/9/2019 1741h £200.8 0.000300 0.00492 Vanadium mg/L 4/5/2019 1023h 4/10/2019 1329h £200.7 0.0150 < 0.0150 Zinc mg/L 4/5/2019 1023h 4/9/2019 1728h £200.8 0.0100 < 0.0100 t f -Analyte(s) were observed above the reporting limit in the filter blank. The filter blank was acceptable, as any associated samples do not have results above the reporting limit/PQL. 2 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD. B -The filter blank was acceptable, as the method blank result is less than 10% of the lowest reported sample concentration. Report Date: 4/11/2019 Page 5 of26 All analyses applicable lo lhe CWA. SOWA. and RCRA are performed m accordance to NELAC protocols Per1inent sampling information is located on the au:,ched COC Confidenlial Business Information: This repon is pro\'ided for the exclusi\ e use of the ~ddressee Pri, ile~>es o~ sub~seq~nt ~,~e of the ~:u:i1e of this .co1~pany or .in~ 1~mbe1 of its stafC, or reproduc1io~ ~f 1h1s repo~ in ~on~u:clion,. \\ith lhe u~~ertisement p~omolio.n 01 sale of ?1!~ ~rodL~cl or p,.ocess, ~r in ~onn~~ion \\ !•h lh~ r~-publication of 1his report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Annual Seeps and Springs 20 I 9 Lab Sample ID: 1903737-001 American West Client Sample ID: Westwater Seep ANALYTICAL LABORATOR IES Collection Date: 3/27/2019 930h Received Date: 3/29/2019 1000h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84 I I 9 Ammonia (as N) mg/L 4/9/201 9 1235h 4/9/2019 1649h E350.I 0.0500 < 0.0500 Bicarbonate (as mg/L 4/2/2019 749h SM2320B 1.00 450 CaC03) Carbonate (as CaC03) mg/L 4/2/2019 749h SM2320B 1.00 < 1.00 Phone: (80 I) 263-8686 Chloride mg/L 4/10/2019 2248h E300.0 5.00 41.6 Toll Free: (888) 263-8686 Fluoride mg/L 4/11/2019 227h E300.0 0.100 0.505 Fax: (801) 263-8687 Ion Balance % 4/10/2019 1356h Cale. -100 0.902 ~-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 3/29/2019 1326h E353.2 0.100 < 0.100 Sulfate mg/L 4/10/2019 2248h E300.0 37.5 436 web: www.awal-labs.com Total Anions, Measured meq/L 4/10/2019 1356h Cale. 19.3 Total Cations, meq/L 4/10/2019 1356h Cale. 19.6 Measured Total Dissolved Solids mg/L 3/29/2019 1145h SM2540C 20.0 1,110 Kyle F. Gross Total Dissolved Solids 4/10/2019 1356h Cale. 0.981 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 4/10/2019 1356h Cale. 1,130 Calculated QA Officer Report Date: 4/11/2019 Page 6 of 26 All anal~ses applic.1ble to the CWA. SOWA. and RCRA we perfom1ed in accordance to NE LAC prolocols Pertinen1 sampling informa1ion is localed on tJ,e al1ached COC Confidential Business Information: This repor1 is provided for the e.~clusi\ e use or1he ~ddressee. P1i \ ile~es o.f su~seq~1enl ~~e of lhe ~'.'1;1e or this .crn~pan~ or rm.\ t~mbe1 of its slnff, or reproducl1~ ~f this repo~ in ~on~ection~ \\ith the a~, er1isemenl. P~?molio.n or sale of ::U!~ ~· od~cl or p1:ocess, ~r in ~onn~c~irn, \\!lh th~ r~·publicotion of this report American West ANALYTICAL LABORATORIES 3440 South 700 West ;alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Annual Seeps and Springs 2019 1903737-00lA Client Sample ID: Westwater Seep Collection Date: 3/27/2019 930h Received Date: 3/29/2019 1000h Analytical Results Analyzed: 3/29/2019 1207h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Dilution Factor: Contact: Tanner Holliday Test Code: 8260-W-DENlOO VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Surr: 1,2-Dichloroethane-d4 17060-07-0 47.8 50.00 95.5 72-151 Surr: 4-Bromofluorobenzene 460-00-4 51.3 50.00 103 80-152 Surr: Dibromofluoromethane 1868-53-7 50.6 50.00 IOI 72-135 Surr: Toluene-d8 2037-26-5 50.8 50.00 102 80-124 Report Date: 4/1 1/2019 Page 7 of 26 All anal~ ses applicable to the CWA, SDWA, and RCRA me perfom1ed in accordance to NELAC protocols Pertinenl sampling information is located on the aliached COC Confidenlial Business. lnfonmuion: This repon is pro, ided for lhe exclusi\ e use oCthe ~ddressee Pri, ile~es o! su~se<f~tenl !'~e of the ~~1e of this .co1~pWl) or .Ul)' ·~~be1 of its slnff or reproducti~ ~f 1h1s repo~ in ~on~eclion_ \\ilh the a~, er1isement p~omotio.n or sale of?'!) ~1odl~CI OJ p,.ocess, ~r in ~onn~c!ion w!lh lh? r~-publication of this report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: April 26, 2019 Company : Address: Contact: Project: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Analytical forAnnual Seeps and Spring 2019 ------- Parameter Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Westwater Seep 475027001 Ground Water 27-MAR-19 09:30 Ol-APR-19 Client Qualifier Result Uncertainty lad Gas Flow Proportional Counting 3FPC, Total Alpha Radium, Liquid "As Received" }ross Radium Alpha U 0.232 +/-0.270 The following Analytical Methods were perfonned: MDC RL 0.982 1.00 Project: Client ID: DNMI00106 DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L JXC9 04/05/19 1228 1863376 ----------------------\1 et hod DescriQ_ti_on _________ _ Analyst Comments EPA 903.0 ;urrogate/Tracer Recovery Test Nominal Recovery% Acceptable Limits ---------Result 3arium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 95 . l (25%-125%) ~otes: :::ounting Uncertainty is calculated at the 68% confidence level (I-sigma). ;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is he greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Seeps and Springs 2019 Lab Sample ID: 1906343-002 Client Sample ID: Ruin Spring Collection Date: 6/11/2019 850h Received Date: 6/13/2019 1054h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Arsenic mg/L 6/14/2019 1410h 6/17/201 9 1351h E200.8 0.00500 < 0.00500 Be1yllium mg/L 6/14/2019 1410h 6/17/2019 153511 E200.8 0.000500 < 0.000500 Cadmium mg/L 6/14/2019 1410h 6/17/2019 1351h E200.8 0.000500 < 0.000500 Calcium mg/L 6/14/2019 1410h 6/28/201 9 1518h E200.7 10.0 165 Phone: (80 I) 263-8686 Chromium mg/L 6/14/201 9 1410h 6/17/2019 1351h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 6/14/2019 141011 6/17/2019 1351h E200.8 0.0100 < 0.0100 Fax: (80 l) 263-8687 Copper mg/L 6/14/2019 1410h 6/17/201 9 1351h E200.8 0.0100 <0.0100 !-mail: awal@awal-labs.com Iron mg/L 6/14/2019 1410h 6/17/2019 1535h E200.8 0.0300 < 0.0300 Lead mg/L 6/14/2019 1410h 6/17/2019 1535h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 6/14/2019 1410h 6/28/2019 1518h E200.7 10.0 45.6 Manganese mg/L 6/14/2019 1410h 6/17/2019 1351h E200.8 0.0100 < 0.0100 Mercury mg/L 6/21/2019 1450h 6/24/2019 752h E245.J 0.000500 < 0.000500 Kyle F. Gross Molybdenum mg/L 6/14/2019 1410h 6/17/2019 1351h E200.8 0.0100 0.0202 LaboratOJ)' Director Nickel mg/L 6/14/2019 141 Oh 6/17/2019 1351h E200.8 0.0200 < 0.0200 Potassium mg/L 6/14/2019 1410h 6/28/2019 1705h E200.7 1.00 3.31 Jose Rocha Selenium mg/L 6/14/2019 1410h 6/17/2019 1351h E200.8 0.00500 0.0108 QA Officer Silver mg/L 6/14/2019 1410h 6/17/2019 1351h E200.8 0.0100 < 0.0100 Sodium mg/L 6/14/2019 1410h 6/28/2019 1518h E200.7 10.0 128 Thallium mg/L 6/14/2019 1410h 6/17/2019 1535h E200.8 0.000500 < 0.000500 Tin mg/L 6/14/2019 14 lOh 6/17/2019 1351h E200.8 0.100 < 0.100 Uranium mg/L 6/14/2019 1410h 6/17/2019 1550h E200.8 0.000300 0.00902 Vanadium mg/L 6/14/2019 1410h 6/28/2019 1705h E200.7 0.0150 < 0.0150 Zinc mg/L 6/14/2019 1410h 6/17/2019 1930h E200.8 0.0100 < 0.0100 Report Date: 7/5/2019 Page 7 of35 All anal~ses applicnl>le 10 the CWA. SOWA. and RCRA rue perfom1ed in accordance to NELAC p1otocols Pertinent sampling i11formalio11 is located on the attached COC C'onl'idenlial Business Information: This 1epor1 is pro, ided for1he e'-.clusi, e use of the ~ddressee Pri,·ile~es or suh~seq~ent ~1;e or lhe ~~e of lhis 0 coi~p1m~ or M) 1~mbe1 of its staff. or reµroductio~ ~'. this repo~ in ~011~ec1ion~ ,, ith the n~\'er1isement p~omo1io.n or sale of ?J!~ ~1 odl~CL or P•.ocess, ~r in :onn:,c~ion w!th th: r:-publication of 1his report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Seeps and Springs 2019 Lab Sample ID: I 906343-002 Client Sample ID: Ruin Spring Collection Date: 6/11/2019 850h Received Date: 6/13/2019 1054h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qua) ,alt Lake City, UT 84119 Ammonia (as N) mg/L 6/23/2019 2000h 6/24/2019 l 127h E350.I 0.0500 < 0.0500 Bicarbonate (as mg/L 6/1712019 739h SM2320B 1.00 202 CaC03) Carbonate (as CaC03) mg/L 6/17/2019 739h SM2320B 1.00 < 1.00 Phone: (80 I) 263-8686 Chloride mg/L 6/28/2019 043h E300.0 1.00 23.9 Toll Free: (888) 263-8686 Fluoride mg/L 6/28/2019 256h E300.0 0.100 0.505 Fax: (80 I) 263-8687 Ion Balance % 6/28/2019 1847h Cale. -100 9.31 !-mail: awal@awal-Jabs.com Nitrate/Nitrite (as N) mg/L 611412019 1048h E353.2 0.100 1.56 Sulfate mg/L 6/27/2019 2139h E300.0 37.5 474 web: www.awal-labs.com Total Anions, Measured meq/L 6/28/2019 1847h Cale. 14.6 Total Cations, meq/L 612812019 1847h Cale. 17.6 Measured Total Dissolved Solids mg/L 6/1412019 I 100h SM2540C 20.0 900 Kyle F. Gross Total Dissolved Solids 6/28/2019 1847h Cale. 0.935 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 612812019 I 847h Cale. 962 Calculated QA Officer Report Date: 7/5/2019 Page 11 of35 All anal) ses applicable to lhe CWA. SOW A. and RCRA are perfom1ed in accordance to NELAC prolocols Pertinent sampling information is located on the aUached COC Conftctenlinl Business Information: This report is pro,•ided for lhe exclusiYe use of lhe ~ddressee Pri, ile~es o.r su~seq~enl ~·~e of 1he ~?1:ne of this .co1~pan) or any 1~'!1be1 of its staff, or reproducli~ ~f this repo~ in ~on~teclion~ wilh the o~, ertisemenl. 11~omoli<>;t1 or sale (lf :11!~ ~rodl~cl or p,.ocess, ~r in ~m1~c~ion ''(th lh~ r~-publication of I his repor1 3440 South 700 West ~alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@av-1al-labs.com web: www.awal-labs.com Kyle F. Gross Laborato1y Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Energy Fuels Resources, Inc. Seeps and Springs 2019 Lab Sample ID: l 906343-002A Client Sample ID: Ruin Spring Collection Date: 6/11/2019 850h Received Date: 6/13/2019 I 054h Analytical Results Analyzed: 6/13/2019 1437h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chlorofonn Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Dilution Factor: Contact: Tanner Holliday Test Code: 8260-W-DENIOO VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < l.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 I 08-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Surr: l ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 51.3 64.8 45.2 51.7 50.00 103 72-151 50.00 130 80-152 50.00 90.3 72-135 50.00 103 80-124 Report Date: 7/5/2019 Page 15 of35 All an.ti) ses applicable Lo lhe CWA. SOWA. and RCRA tue performed in accordance lo NELAC protocols Pertinent sampling information is located on tile attached COC C'onfidenLinl Business lnformnrion: This report is p1cn·tded for lhe exclusire use of the ~ddressee Pt i, ile~es o,r sub,..5eq~enl ~·~e or the ~?',lle of lhis .co1~pan~ or M) 1~7mbe1 or ils staff, or reproduclio~ ~f Lh1s repo~ in ~011~1eclion~ "ilh the a~, er1isemenl p~omolio.n or sale of ru!~ ~1odt~cl or P•.ocess, ~r in ~onn:_c~ion "~th 1h; r:-publica1io11 of this report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: July 8, 2019 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Project: Analytical forSeeps and Springs 2019 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Ruin Spring 481772002 Ground Water l l-JUN-19 08:50 13-JUN-l 9 Client Parameter Qualifier Result Uncertainty lad Gas Flow Proportional Counting }FPC, Total Alpha Radium, Liquid "As Received" }ross Radium Alpha U -0.116 +/-0.106 The following Analytical Methods were performed: MDC 0.642 RL 1.00 Project: Client ID: DNMI00106 DNMI001 Units PF DF Analyst Date Time Batch Method pCi/L LXB3 06/28/19 1148 1888588 \.f~e~th~o~d _______ D_e_sc_r_.i _t_io_n _____________________ A~n~a~l st Co~m=m~e=nt~s __________ _ EPA 903.0 iurrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 3arium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 90.6 (25%-125%) lfotes: :ounting Uncertainty is calculated at the 68% confidence level (I-sigma). iRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is he greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Seeps and Springs 2019 Lab Sample ID: 1906343-001 American West Client Sample ID: Entrance Seep ANALYTICAL LABORATOR I ES Collection Date: 6/11/2019 815h Received Date: 6/13/2019 1054h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84119 Arsenic mg/L 6/14/2019 1410h 6/17/2019 1342h E200.8 0.00500 0.00894 Beryllium mg/L 6/14/2019 1410h 6/17/2019 1448h E200.8 0.000500 < 0.000500 Cadmium mg/L 6/14/2019 1410h 6/17/2019 1342h E200.8 0.000500 < 0.000500 Calcium mg/L 6/14/2019 1410h 6/28/2019 1507h E200.7 10.0 155 Phone: (801) 263-8686 Chromium mg/L 6/14/2019 1410h 6/17/2019 1342h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 6/14/2019 1410h 6/17/2019 1342h E200.8 0.0100 < 0.0100 Fax: (80 I) 263-8687 Copper mg/L 6/14/2019 1410h 6/17/2019 1342h E200.8 0.0100 < 0.0100 !-mail: awal@awal-labs.com Iron mg/L 6/14/2019 1410h 6/17/2019 1448h E200.8 0.0300 0.453 Lead mg/L 6/14/2019 1410h 6/17/2019 1448h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 6/14/2019 1410h 6/28/2019 1507h E200.7 10.0 48.0 Manganese mg/L 6/14/2019 1410h 6/J 7/2019 1342h E200.8 0.0100 0.587 Mercury mg/L 6/21/2019 1450h 6/24/2019 758h E245.l 0.000500 < 0.000500 Kyle F. Gross Molybdenum mg/L 6/14/2019 14 JOh 6/17/2019 1342h E200.8 0.0100 0.01.43 Laboratory Director Nickel mg/L 6/14/2019 1410h 6/17/2019 1342h E200.8 0.0200 < 0.0200 Potassium mg/L 6/14/2019 1410h 6/28/2019 1703h E200.7 1.00 4.66 Jose Rocha Selenium mg/L 6/14/2019 1410h 6/17/2019 1342h E200.8 0.00500 < 0.00500 QA Officer Silver mg/L 6/14/2019 1410h 6/17/2019 1342h E200.8 0.0100 < 0.0100 Sodium mg/L 6/14/2019 1410h 6/28/2019 1507h E200.7 10.0 126 Thallium mg/L 6/14/2019 1410h 6/17/2019 1448h E200.8 0.000500 < 0.000500 Tin mg/L 6/14/2019 1410h 6/17/2019 1342h E200.8 0.100 <0.100 Uranium mg/L 6/14/2019 1410h 6/17/2019 1547h E200.8 0.000300 0.0701 Vanadium mg/L 6/14/2019 1410h 6/28/2019 1703h E200.7 0.0150 < 0.0150 Zinc mg/L 6/14/2019 1410h 6/17/2019 1927h E200.8 0.0100 < 0.0100 2 -Analyte concentration is too high/or accurate matrix spike recovery and/or RPD. Report Date: 7/5/2019 Page 6 of 35 All anal~ses applicable lo the CWA. SOWA. and RCRA are perfomled in accordance Lo NELAC protocols Pe11inent sampling information is located on lhe atlached COC Confidential Business Information: This report is pro, ided for lhe exclusiYe use of 1he ~ddressee Pri, ile~es o~ subpsec1~1ent ~,~e of the ~~1e of this .co1~pan~ or M) 1~mbe1 of its slaff, or reproduclio!~ ~f this repo~ in ~on~1ecli01~ \\ith 1he n~,enisemenL P~?moti~n 01 sale of?'!) ~1odL~CI or P•.ocess, ~1 in ~onn~c!ion '''!th lh~ r~·publication of this repcirl INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Seeps and Springs 2019 Lab Sample ID: 1906343-00 I American West Client Sample ID: Entrance Seep ANALYTICAL LABORATORIES Collection Date: 6/11/2019 815h Received Date: 6/13/2019 1054h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84 I 19 Ammonia (as N) mg/L 6/23/2019 2000h 6/24/2019 1120h E350.l 0.0500 0.168 Bicarbonate (as mg/L 6/17/2019 739h SM2320B 1.00 480 CaC03) Carbonate (as CaC03) mg/L 6/J 7/2019 739h SM2320B 1.00 < 1.00 Phone: (801)263-8686 Chloride mg/L 6/27/2019 2016h E300.0 1.00 104 Toll Free: (888) 263-8686 Fluoride mg/L 6/28/2019 346h E300.0 0.100 0.912 fax: (80 I) 263-8687 Ion Balance % 6/28/2019 1847h Cale. -100 4.46 !-mail : awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 6/J 4/2019 1110h E353.2 0.100 < 0.100 Sulfate mg/L 6/27/2019 2016h E300.0 7.50 160 web: www.awal-labs.com Total Anions, Measured meq/L 6/28/2019 1847h Cale. 15.9 Total Cations, meq/L 6/28/2019 1847h Cale. 17.4 Measured Total Dissolved Solids mg/L 6/14/2019 I JOOh SM2540C 20.0 892 @ Kyle F. Gross Total Dissolved Solids 6/28/2019 1847h Cale. 1.01 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 6/28/2019 1847h Cale. 887 Calculated QA Officer @ -High RPD due to suspected sample non-homogeneity or matrix interference. 1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Report Date: 7/5/2019 Page 10 of35 All anal~ ses applicnllle lo lhe CW A. SOWA and RCRA a1e perfomted in accordance to NELAC protocols Pertinent sampling informal ion is located on Lhe attached COC Conlidentiol Business lnformalion: This repon is pro\'ided for the exclusi, e use of the ~cldressee Pri, ile~es or su~se<1~1en1 ~,~e or lhe ~~1e of this .co1~pan~ 01 an~ 1~~mber or its slaff, or re1>roducti~ ~r this repo~ in _con~eclion .. ,,i1h the a~, ertisement. P~?moti~n o, sale of?'!~ ~rod~cl or p~ocess, ~r in ~onn':~ion "!'h th~ r~-publication of this repor1 3440 South 700 West ,alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle f. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Energy Fuels Resources, Inc. Seeps and Springs 2019 Lab Sample ID: l 906343-00 I A Client Sample ID: Entrance Seep Collection Date: 6/ 11/2019 815h Received Date: 6/13/2019 1054h Analytical Results Analyzed: 6/13/2019 1417h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Dilution Factor: Contact: Tanner Holliday Test Code: 8260-W-DENlOO VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 5.59 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 J 7060-07-0 460-00-4 1868-53-7 2037-26-5 56.3 53.1 51.1 50.6 50.00 113 72-151 50.00 106 80-152 50.00 102 72-135 50.00 101 80-124 Report Date: 7/5/2019 Page 14 of35 All annl~ses ap1>licable to the CWA. SOWA. and RCRA ,ue flerformed in accordance lo NELAC protocols Pertinenl srunpling information is located on the nUached COC Confidenlml Business Information: TI1is report is 1>ro, 1ded for the exclusi, e use of the ~ddressee Pri, ile~es o~ sub__seq~ent ~,~e or the ~~1e of I his .co11_1pnny or an~ ~mbet of ils sl:tIT. or reproduc1i~ ~f this repo~ in ~on~1eclion .. ,,ith the u~, ertisement. p~omoti~n 01 sale of?'!~ ~1odl~CI or p1.ocess. ~r in ~onn~~ion \\'!th lh~ r~-publicalion or this report Company: Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Analytical forSeeps and Springs 2019 ----------Entrance Seep 481772001 Ground Water 11-JUN-19 08:15 13-JUN-19 Client Project: Client ID: Report Date: DNMI00106 DNMIOOl July 8, 2019 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method lad Gas Flow Proportional Counting :iFPC, Total Alpha Radium, Liquid "As Received" }ross Radium Alpha 2.63 +/-0.455 0.947 1.00 pCi/L LXB3 06/28/19 1148 1888588 The following Analytical Methods were performed: -----------------\1 et hod Descri tion Anal st Comments EPA 903.0 ;urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits ---------------------------~----'-----3 a r i um Carrier GFPC, Total Alpha Radium, Liquid "As Received" 89.9 (25%-125%) 'fotes: =:ounting Uncertainty is calculated at the 68% confidence level (I-sigma). ;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is he greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Seeps and Springs 2019 Lab Sample ID: l 906343-003 Client Sample ID: Cottonwood Spring Collection Date: 6/11/2019 950h Received Date: 6/13/2019 1054h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual :;alt Lake City, UT 84119 Arsenic mg/L 6/14/2019 141 Oh 6/17/2019 1401h E200.8 0.00500 < 0.00500 Beryllium mg/L 6/14/2019 1410h 6/17/2019 1454h E200.8 0.000500 < 0.000500 Cadmium mg/L 6/14/2019 1410h 6/17/2019 1401h E200.8 0.000500 < 0.000500 Calcium mg/L 6/14/2019 1410h 6/28/2019 1527h E200.7 10.0 122 Phone: (80 I) 263 -8686 Chromium mg/L 6/14/2019 1410h 6/17/2019 1401h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 6/14/2019 1410h 6/17/2019 1401h E200.8 0.0100 < 0.0100 Fax: (801) 263-8687 Copper mg/L 6/14/2019 141 Oh 6/17/2019 1401h E200.8 0.0100 < 0.0100 ~-mail: awal@awal-labs.com Iron mg/L 6/14/2019 1410h 6/17/2019 1454h E200.8 0.0300 < 0.0300 Lead mg/L 6/14/2019 1410h 6/17/2019 1454h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 6/14/2019 1410h 6/28/2019 1527h E200.7 10.0 35.3 Manganese mg/L 6/14/2019 1410h 6117/2019 1401h E200.8 0.0100 < 0.0100 Mercury mg/L 6/21/2019 1450h 6/24/2019 800h E245.l 0.000500 < 0.000500 Kyle F. Gross Molybdenum mg/L 6/14/2019 1410h 6/17/2019 1401h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 6/14/2019 14 IOh 6/17/2019 1401h E200.8 0.0200 < 0.0200 Potassium mg/L 6/14/2019 1410h 6/28/2019 1712h E200.7 1.00 6.78 Jose Rocha Selenium mg/L 6/14/2019 1410h 6/17/2019 1401h E200.8 0.00500 < 0.00500 QA Officer Silver mg/L 6/14/2019 1410h 6/17/2019 1401h E200.8 0.0100 < 0.0100 Sodium mg/L 6/14/2019 1410h 6/28/2019 1527h E200.7 10.0 268 Thallium mg/L 6/14/2019 1410h 6/17/2019 1454h E200.8 0.000500 < 0.000500 Tin mg/L 6/14/2019 1410h 6/17/2019 1401h E200.8 0.100 < 0.100 Uranium mg/L 6/14/2019 1410h 6/17/2019 1553h E200.8 0.000300 0.0101 Vanadium mg/L 6/14/2019 1410h 6/28/2019 1712h E200.7 0.0150 < 0.0150 Zinc mg/L 6/14/2019 1410h 6/17/2019 1939h E200.8 0.0100 < 0.0100 Report Date: 7/5/2019 Page 8 of35 All Mal~ses applicable lo the CWA, SOWA. and RCRA are performed in accordance to NELAC prolocols Pe11inent sampling information is located on 1he allached COC Conlidenlial Business lnfounalion: This report is provided for theexdusi,e use of the ~ddressee Pri, ile~es o~su~seq~enl ~J~e or the ~~1e of this .co1~pa11:,. or .in) ~mbet ofils sc:iff, or reproductio~ ~f this repo~ in .con~1eclion~ \\ilh the n~,erlisement. p~omoli~n or sale of~!~ ~todL~cl or p1.ocess, ~r in ~nm;c!ion "'.th 1h~ r~-publication of this repor1 INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Seeps and Springs 2019 Lab Sample ID: 1906343-003 American West Client Sample ID: Cottonwood Spring ANALYTICAL LABORATORIES Collection Date: 6/11/2019 950h Received Date: 6/13/2019 1054h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual falt Lake City, UT 84119 Ammonia (as N) mg/L 6/23/2019 2000h 6/24/2019 1128h E350.l 0.0500 < 0.0500 Bicarbonate (as mg/L 6/17/2019 739h SM23208 1.00 286 CaC03) Carbonate (as CaC03) mg/L 6/17/2019 739h SM23208 1.00 < 1.00 Phone: (80 I) 263 -8686 Chloride mg/L 6/27/2019 2156h E300.0 5.00 138 Toll Free: (888) 263-8686 Fluoride mg/L 6/28/2019 403h E300.0 0.100 0.249 Fax: (80 I) 263-8687 Ion Balance % 6/28/2019 1847h Cale. -100 6.19 ~-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 6/14/2019 llllh E353.2 0.100 < 0.100 Sulfate mg/L 6/27/2019 2156h E300.0 37.5 423 web: www.awal-labs.com Total Anions, Measured meq/L 6/28/2019 1847h Cale. 18.4 Total Cations, meq/L 6/28/2019 1847h Cale. 20.9 Measured Total Dissolved Solids mg/L 6/14/2019 1100h SM2540C 20.0 1,010 Kyle F. Gross Total Dissolved Solids 6/28/2019 1847h Cale. 0.868 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 6/28/2019 1847h Cale. 1,170 Calculated QA Officer Report Date: 7/5/2019 Page 12 of35 All analyses a1>plicable lo lhe CW A. SDWA. and RCRA are perfom1ed in accordance to NELAC protocols Pertinent sampling infonnalion is locnted on the attached COC C'onlidentiol Business Information: This 1epor1 is plO\ ided for lhe exclusi, e use of the ~ddressee Pri, ile~es of su~seq~1enl ~~e ol"the ~~1e of this .con:1pnn~ or an~ ~mbe1 of its stMT. or reproductio~ ~f this repo~ in ~01~1eclion~ \\ith then~, ertisemen1 p~omolio.n 01 sale of :11!~ ~1odl~CI or p1.ocess, ~r in ~nn~c!ion w!lh 1h~ r~-publication of this 1eporl American West ANALYTICAL LABORATORIES 3440 South 700 West ;alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Energy Fuels Resources, Inc. Seeps and Springs 2019 Lab Sample ID: l 906343-003A Client Sample ID: Cottonwood Spring Collection Date: 6/11/2019 950h Received Date: 6/13/2019 1054h Analytical Results Analyzed: 6/13/2019 1457h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Dilution Factor: Contact: Tanner Holliday Test Code: 8260-W-DENIOO VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Surr: l ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 51.2 54.5 45.5 50.6 50.00 102 72-151 50.00 109 80-152 50.00 91.0 72-135 50.00 101 80-124 Report Date: 7/5/2019 Page 16 of35 All analyses applicable Lo lhe CWA. SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is localed on Lhe allached COC ConfidenLiul Business Information: This report is prm ided for lhe exclusi, e use or the ~ddressee. P1i, ile~es o.r sub...5eq~ent ~·~e of Lhe ~~1e of [his .co11:1pan~ or an~ 1~mbe1 of its slaff. or reproduclio~ ~f Lhis repo1; in .con?ection~ ,,ith then~, ertisement. P~?moli~n 01 sale of~!) rrod~cl or p1.ocess, ~r in ~onn1;_c~Lon '''!th lh~ r~-publicalion of Lhis report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: Analytical forSeeps and Springs 2019 ------------Client Sample ID: Cottonwood Spring Sample ID: 481772003 Matrix: Ground Water Collect Date: l l-JUN-19 09:50 Receive Date: 13-JUN-19 Collector: Client Project: Client ID: Report Date: DNMI00106 DNMI001 July 8, 2019 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method ----------------~--------------lad Gas Flow Proportional Counting }FPC, Total Alpha Radium, Liquid "As Received" }ross Radium Alpha U 0.393 +/-0.257 0.833 1.00 pCi/L LXB3 06/28/19 1149 1888588 The following Analytical Methods were performed: \1ethod Description Analyst Comments EPA 903.0 ;urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits ---------------3arium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 76. 6 (25%-125%) llotes: :::ounting Uncertainty is calculated at the 68% confidence level (I-sigma). ;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is he greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: OF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Seeps and Springs 2019 Lab Sample ID: 1906343-004 Client Sample ID: Back Spring Collection Date: 6/11/2019 850h Received Date: 6/13/2019 1054h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Arsenic mg/L 6/14/2019 1410h 6/17/2019 1404h E200.8 0.00500 < 0.00500 Beryllium mg/L 6/14/2019 1410h 6/17/2019 1508h E200.8 0.000500 < 0.000500 Cadmium mg/L 6/14/2019 1410h 6/17/2019 1404h E200.8 0.000500 < 0.000500 Calcium mg/L 6/14/2019 1410h 6/28/2019 1529h E200.7 10.0 157 Phone: (80 I) 263-8686 Chromium mg/L 6/14/2019 1410h 6/17/2019 1404h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 6/14/2019 1410h 6/17/2019 1404h E200.8 0.0100 < 0.0100 Fax: (801) 263-8687 Copper mg/L 6/14/2019 1410h 6/17/2019 1404h E200.8 0.0100 < 0.0100 ~-mail: awal@awal-labs.com Iron mg/L 6/14/2019 1410h 6/17/2019 1508h E200.8 0.0300 < 0.0300 Lead mg/L 6/14/2019 141 Oh 6/17/2019 1508h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 6/14/2019 14 !Oh 6/28/2019 1529h E200.7 10.0 35.7 Manganese mg/L 6/14/2019 1410h 6/17/2019 1404h E200.8 0.0100 < 0.0100 Mercury mg/L 6/21/2019 1450h 6/24/2019 802h E245.l 0.000500 < 0.000500 Kyle F. Gross Molybdenum mg/L 6/14/2019 1410h 6/17/2019 1404h E200.8 0.0100 0.0187 Laboratory Director Nickel mg/L 6/14/2019 1410h 6/17/2019 1404h E200.8 0.0200 < 0.0200 Potassium mg/L 6/14/2019 1410h 6/28/2019 1715h E200.7 1.00 3.30 Jose Rocha Selenium mg/L 6/14/2019 1410h 6/17/2019 1404h E200.8 0.00500 0.00961 QA Officer Silver mg/L 6/14/2019 1410h 6/17/2019 1404h E200.8 0.0100 < 0.0100 Sodium mg/L 6/14/2019 1410h 6/28/2019 1529h E200.7 10.0 119 Thallium mg/L 6/14/2019 1410h 6/17/2019 1508h E200.8 0.000500 < 0.000500 Tin mg/L 6/14/2019 1410h 6/17/2019 1404h E200.8 0.100 < 0.100 Uranium mg/L 6/14/2019 1410h 6/17/2019 1557h E200.8 0.000300 0.00901 Vanadium mg/L 6/14/2019 1410h 6/28/2019 1715h E200.7 0.0150 < 0.0150 Zinc mg/L 6/14/2019 1410h 6/17/2019 1943h E200.8 0.0100 < 0.0100 Report Date: 7/5/2019 Page 9 of35 All anal~ses applicable Lo lhe CWA. SOWA. and RCRA are performed m accordance to NELAC protocols Pertinent sampling information is located on the allached COC Confidential Business Information: TI1is report is prm ided for the exclusi, e use of lhe ~ddressee Pri\ ile~es o.r sub}eq~enl ~~e of the ~~1e of lhis .co1~pan~ or an~ 1~mbe1 of its slaff, or reproductio~ ~f I his repm; in .con~tection~ \\ilh the a~, ertisement p~omotio.n OI saJe of ?1!). rrodL!CL or p~ocess. ~r in :onm~c~ion \\ !lh lh~ rr::-publication or this repor1 INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Seeps and Springs 2019 Lab Sample ID: 1906343-004 Client Sample ID: Back Spring Collection Date: 6/11/2019 850h Received Date: 6/13/2019 1054h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ~alt Lake City, UT 84119 Ammonia (as N) mg/L 6/23/2019 2000h 6/24/2019 1129h E350.J 0.0500 < 0.0500 Bicarbonate (as mg/L 6/17/2019 739h SM2320B 1.00 202 CaC03) Carbonate (as CaC03) mg/L 6/17/2019 739h SM2320B 1.00 < 1.00 Phone:(801)263-8686 Chloride mg/L 6/28/2019 100h E300.0 1.00 23.7 Toll Free: (888) 263-8686 Fluoride mg/L 6/28/2019 420h E300.0 0.100 0.460 Fax: (80 I) 263-8687 Ion Balance % 6/28/2019 1847h Cale. -100 6.06 ~-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 6/14/2019 1051h E353.2 0.100 1.65 Sulfate mg/L 6/27/2019 2213h E300.0 37.5 455 web: www.awal-labs.com Total Anions, Measured meq/L 6/28/2019 1847h Cale. 14.2 Total Cations, meq/L 6/28/2019 1847h Cale. 16.1 Measured Total Dissolved Solids mg/L 6/14/2019 1100h SM2540C 20.0 816 Kyle F. Gross Total Dissolved Solids 6/28/2019 1847h Cale. 0.889 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 6/28/2019 1847h Cale. 918 Calculated QA Officer Report Date: 7/5/2019 Page 13 of35 All anal~ses applicable to lhe (WA. SDWA. and RCRA are perfonned in accordance to NELAC p1olocols Pertinenl sampliny informulion is located on lhe aU.iched COC C'onfidentinl Business lnformulion: This repor1 is provided for the exclusi\e use of lhe ~ddressee P1i, ile~es of su~seq~1enl ~'!e of the ~:11;1e of this .con_,p•m~ or rtn} r~mbe1 or its slnff. or reproduclio~ ~r this repo~ in ~on~t~lion .. \\ith lhe ll~\ ertisement P~?motio.n or sale of ~lY ~tOdl~CI or p1 0 ocess, ?r in ;0nm;.c~ion ,\ }th 1h~ r~·publicotion of this 1eport ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Seeps and Springs 2019 l 906343-004A American West Client Sample ID: ANALvT1cAL LAeoRAToR1Es Collection Date: Back Spring 6/11/2019 850h 3440 South 700 West ~alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax:(801 )263-8687 ~-mail : awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Received Date: 6/13/2019 1054h Analytical Results Analyzed: 6/13/2019 1517h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surrogate Units: µg/L Surr: l,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-dB Dilution Factor: CAS 17060-07-0 460-00-4 1868-53-7 2037-26-5 Contact: Tanner Holliday Test Code: 8260-W-DENlOO VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Result Amount Spiked %REC Limits Qual 51.4 50.00 103 72-151 55.2 50.00 110 80-152 45.6 50.00 91.3 72-135 51.5 50.00 103 80-124 Report Date: 7/5/2019 Page 17 of35 All anal~ ses a1>i,licrible 10 lhe CWA. SOWA~ and RCRA me perlom1ed in accordRnce to NELAC prolocols Pertmenl sampling information is located on Ll1e auached COC Conl'identinl Business Information: This re1>0r1 is provided for the e.xcluSi\e use or the ~ddressee Pri, i le~es o: sub .. seq~ent ~~e of lhe ~~e of lhis .co':1prm~ or nny 1~mbe1 of its slafT. or reproduclio~ ~f this repo~ in .con~lec11on .. " ilh lhe n~, ertisement p~omotio.n or sale or~!~ ~rod~cl or p1.ocess, ~1 in ~nn:_c!ion w~th th; r:-publicotion of this 1eporl Company: Address: Contact: Project: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Analytical forSeeps and Springs 2019 Report Date: July 8, 2019 ----------------------Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Back Spring 481772004 Ground Water 1 l-JUN-19 08:50 13-JUN-19 Client Project: Client ID: DNMI00106 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method "--------------lad Gas Flow Proportional Counting }FPC, Total Alpha Radium, Liquid "As Received" }ross Radium Alpha U 0.201 +/-0.158 0.545 1.00 pCi/L LXB3 07/02/19 0613 1888588 The following Analytical Methods were perfonned: \1ethod Description Analyst Comments EPA 903.0 ;urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 3arium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 91.3 (25%-125%) lfotes: :ounting Uncertainty is calculated at the 68% confidence level (I-sigma). ;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is he greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Annual Seeps and Springs 2019 1903737-002A Client Sample ID: Trip Blank ANALYTICAL LAB0RAT0R1Es Collection Date: 3/27/2019 930h 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Received Date: 3/29/2019 1000h Analytical Results Analyzed: 3/29/2019 1227h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Dilution Factor: Contact: Tanner Holliday Test Code: 8260-W-DENIOO VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Jose Rocha QA Officer Surr: l,2-Dichloroethane-d4 Surr: 4-Bromotluorobenzene Surr: Dibromotluoromethane Surr: Toluenc-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 48.5 52.2 50.5 51.2 50.00 97.0 72-151 50.00 104 80-152 50.00 IOI 72-135 50.00 102 80-124 Report Date: 4/11/2019 Page 8 of26 All anal~ses applicnble to the CWA. SOWA. and RCRA me perfom,ed in accordance to NELAC prolocols, Pe1tinenl sampling i1,ronnDlion is locr1ted on lhe altached COC. Confidential Business Jnfonnation: This repor1 is pro, ided for the exclush e use oflhe ~ddressee P1i\ ile~es o.f sub .. sec,~enl ~1~e or lhe ~~e or this 0 co1~po.n~ or M) 1~mbe1 or its slaff, or reproducti~ ~f this repo~ in .con~1ec11on~ ,\11h the <I~\ er1isement. p~omo1i~ or sale of~!~ ~rodllCl or p~ocess, ?r in ~nn~c~ion \\ !'h lh~ r~-publica1ion of this repor1 ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. Seeps and Springs 2019 1906343-005A American West Client Sample ID: Trip Blank ANALYTICAL LAeoRAToA1es Collection Date: 6/11/2019 815h 3440 South 700 West ,alt Lake City, UT 84119 Phone: (801 ) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Received Date: 6/13/2019 Analytical Results Analyzed: 6/13/2019 1357h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surrogate Units: µg/L Surr: l ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 1054h Dilution Factor: CAS 17060-07-0 460-00-4 1868-53-7 2037-26-5 Contact: Tanner Holliday Test Code: 8260-W-DENIOO VOAs by GC/MS Method 8260C/5030C Method: SW8260C CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Result Amount Spiked %REC Limits Qual 50.9 50.00 102 72-151 53.9 50.00 108 80-152 45.4 50.00 90.9 72-135 50.2 50.00 100 80-124 Report Date: 7/5/2019 Page 18 of35 All annl~ ses applicnble to lhe C'WA. SOWA_ Md RCRA are perfom,ed in accordance 10 NELAC protocols. Peninent sampling infonnation is Jocnted on tJ1e altached COC Coniiden1inl Business Information: This report is provided for 1he exclusi\e use of the ~ddressee Pri, ile~es o: sub .. seq~enl ~·~e or Lhe ~:'1.'1e of this .con,ipnn~ or M) 1~mbe1 of ils slalT. or reproductio1~ ~: lh1s repm; in .cot)?tction ... \\ilh the a~, er1iseme111 p~omoti~n ~r sale of~!~. ~rod~cl or P•.?cess, ~r in ~nn:_c~ion w!th th~ r1;-publicutio11 of this repor1 American West ANALYTICAL LABORATORIES 3440 South 700 West ;alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail : awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Tanner Holliday Energy Fuels Resources, Inc. 6425 South Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: Annual Seeps and Springs 2019 Dear Tanner Holliday: Lab Set ID: 1903737 American West Analytical Laboratories received sample(s) on 3/29/2019 for the analyses presented in the following report. American West Analytical Laboratories (AW AL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, Wyoming, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Approved by: K I F Digitally signed y e . by Kyle F. Gross Date: Gross 2019.04.11 15:39:22 -06'00' Laboratory Director or designee Report Date: 4/11/2019 Page I of26 All anal~ ses applicnble to lhe CWA. SOWA. and RCRA are performed in accordance lo NELAC protocols Per1inent sampling informolion is locnled on lhe allached COC Conridenliol Business lnformalion: This report is pro,ided for lhe exclusiH use oflhe ~ddressee Pri, ile~es of sub .. seq~1enl ~~e or lhe ~~i:: or this .co1~pan~ or an~ 1~:mbe1 of ils staff. or reproduclio~ ~~ this repo~ in 0 C011)1ection~ \\ilh the a~, e11isemenl. P~?motio.n or sale or :U!> ~rodi~t or p~ocess, ~r in ~nm~.c!ion w~lh th~ r~·publication or 1his report 3440 South 700 West ;alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer SAMPLE SUMMARY Client: Project: Lab Set ID: Energy Fuels Resources, Inc. Annual Seeps and Springs 2019 1903737 Date Received: 3/29/2019 1 OOOh Lab Sample ID Client Sample ID Date Collected 1903737-00lA Westwater Seep 3/27/2019 930h 1903737-00IB Westwater Seep 3/27/2019 930h 1903737-00lB Westwater Seep 3/27/2019 930h 1903737-00lC Westwater Seep 3/27/2019 930h 1903737-00ID Westwater Seep 3/27/2019 930h 1903737-00ID Westwater Seep 3/27/2019 930h 1903737-00lE Westwater Seep 3/27/2019 930h 1903737-00IE Westwater Seep 3/27/2019 930h 1903737-00lE Westwater Seep 3/27/2019 930h 1903737-00 IE Westwater Seep 3/27/2019 930h l 903737-002A Trip Blank 3/27/2019 930h Contact: Tanner Holliday Matrix Analysis Aqueous VOA by GC/MS Method 8260C/5030C Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level Aqueous Anions, E300.0 Aqueous Total Dissolved Solids, A2540C Aqueous Ammonia, Aqueous Aqueous Nitrite/Nitrate (as N), E353.2 Aqueous Mercury, Drinking Water Dissolved Aqueous ICPMS Metals, Dissolved Aqueous ICP Metals, Dissolved Aqueous Ion Balance Aqueous VOA by GC/MS Method 8260C/5030C Report Date: 4/11/2019 Page 2 of 26 All anal~ ses applicnble lo lhe CWA. SOWA. and RCRA are perfom1ed in accordance to NELAC protocols Pertinenl sampling informalion is located 011 Lhe allached COC Confidential Business Jnformaliotr This repor1 is prO\'ided for lhe exclusirn use of 1he ~ddressee Pri, ile~es o~ su~seq~enl ~·~e of the ~~ne of lhis .co,~p:m~ or an~ 1~mber of its slafT. or reproduclior~ ~f I his repo~ in ~on~1ec1ion~ \\ith the a~, ertisemenl p~~moli<>;" or sale of :1'!~ ~roch~I or p~ocess, ~r in ~nn~c!ion "!'h lh~ r~-publication of lhis r~port 3440 South 700 West ;aft Lake City, UT 84 I 19 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail : awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: Annual Seeps and Springs 2019 1903737 3/29/2019 3/27/2019 Intact See Chain of Custody Holding Time and Preservation Requirements: The analysis and preparation for the samples were performed within the method holding times. The samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPO, DUP: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination, with the following exceptions: Zinc and Manganese were observed above the reporting limit in the filter blank MB-FIL TER-61769. The blank was acceptable, as any associated samples do not have results above the reporting limits. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike / Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exceptions: Sam le ID Anal e QC 1903737-00lE Sodium MSD Duplicate (DUP): The parameters that required a duplicate analysis had RPDs within the control limits. Corrective Action: None required. Report Date: 4/11/2019 Page 3 of 26 All annl~ses applicable lo the CWA SOWA. and RCRA are perfom1ed in accordance to NELAC prolocols Pertinent sampling information is located on the all:iched COC Confidential Business lnfornuilion: This repon is pro,·ided for 1he exclusi\e use ofthl" ~ddressee Pri, ile~es of sub .. seci~1ent ~;e or the ~:":'le of lhis .co,~puny or an~ t~mber of ils st:1ff. or reproduclio~ ~( this repo~ in ~on~1ec1ion ... with the a~, ertisemenL P~?mori~n or sale of?'!) ~rodL~cl or p~oces~, ~r in ~onn~c~ion \\ !th 1h~ r~-publication of this reporl 3440 South 700 West ~alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 !-mail : awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: Method: Analysis: Annual Seeps and Springs 2019 1903737 3/29/2019 3/27/2019 Intact See Chain of Custody SW-846 8260C/5030C Volatile Organic Compounds General Set Comments: No target analytes were observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPO, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike / Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 4/11/2019 Page 4 of26 All an:il) ses applicable to the CW A4 SOW A. and RCRA are per(om1ed in accordance to NELAC protocols Pertinenl sampling information is located on the auached COC Confidential Business lnformalion: This report is pro\ ided for lhe exclusi\e use or lhe ~ddressee Pri, ile~es or su~seq~enl ~1;e or lhe ~~e of lhis .cm~pan~ or an) ~mber of ils starr. or reproducli~ ~f lhis repo~ in ~Ol~leclion~ \\ith lhe :)~vertisemenl. p~~moli°!1 or sale of ?'!Y ~rodL~CI or p~ocess, ~· in ~onn~c!ion \\'!th th~ r~-publication of lhis ,~port American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. LabSetlD: 1903737 Project: Annual Seeps and Springs 2019 Analyte Result Lab Sample ID: LCS-61799 Date Analyzed: Test Code: 200.7-DIS Date Prepared: - Calcium 11.0 Magnesium 11.2 Potassium I I.I Sodium I I.I Vanadium 0.218 Lab Sample ID: LCS-61800 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Arsenic 0.198 Beryllium 0.198 Cadmium 0.192 Chromium 0.200 Cobalt 0.195 Copper 0.196 Iron 0.992 Lead 0.180 Manganese 0.200 Molybdenum 0.191 Selenium 0.197 Thallium 0.177 Tin 0.967 Uranium 0.196 Lab Sample ID: LCS-61800 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Nickel 0.189 Silver 0.194 Zinc 0.961 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Units Method 04/10/20191314h 04/05/2019 I 023h mg/L E200.7 mg/L E200 7 mg/L E200.7 mg/L E200.7 mg/L E200.7 04/08/2019 1221h 04/05/2019 1023h mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200 8 mg/L E200 8 mg/L E200.8 mg/L E200 8 mg/L E200.8 mg/L E200,8 mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200,8 mg/L E200.8 04/09/2019 1725h 04/05/2019 1023h mg/L E200.8 mg/L E200.8 mg/L E200,8 MDL 0.0937 0.0439 0.134 0.187 0.00138 0.000298 0.000198 0.0000858 0.00191 0.000300 0.00282 0.0496 0.000448 0.00108 0.000652 0.000574 0.000154 0.00116 0.000176 0.00148 0.000232 0.00418 Reporting Limit 1.00 1.00 1.00 1.00 0.00500 0.00200 0.00200 0.000500 0.00200 0.00400 0.00200 0.100 0.00200 0.00200 0.00200 0.00200 0.00200 0.00400 0.00200 0.00200 0.00200 0.00600 Contact: Dept: QC Type: Amount Spiked 10.00 10.00 10.00 10.00 0.2000 0.2000 0.2000 0.2000 0.2000 0.2000 0.2000 1.000 0.2000 0.2000 0.2000 0.2000 0.2000 1.000 0.2000 0.2000 0.2000 1.000 Tanner Holliday ME LCS Spike Ref. Amount 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 %REC 110 112 Ill Ill 109 98.8 99.2 96.2 99.9 97.4 97.9 99.2 90.1 99.8 95.6 98.5 88.7 96.7 97.8 94.6 97.0 96.1 Limits 85 -115 85 -115 85 -115 85 -115 85 -115 85 -115 85 -115 85 -115 85 -115 85 -115 85 -115 85 -115 85 -l l 5 85 -115 85 -115 85 -115 85 -115 85 -115 85 • 115 85 • 115 85 • 115 85 • 115 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 4/11/2019 Page 9 of 26 analyses applicable to the CWA. SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling infom,ation is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tl- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee \\rill be granted only on contact. This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1903737 Project: Annual Seeps and Springs 2019 Analyte Result Lab Sample ID: LCs-61789 Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury 0.00361 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awai-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 04/10/2019 824h 04/04/2019 1830h mg/L E245.I 0.0000396 0.0000900 0.003330 - Tanner Holliday ME LCS Spike Ref. Amount %REC 0 108 - Limits 85 -115 ---- Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPO Limit Qual Report Date: 4/11/2019 Page 10 of26 analyses applicable to the CWA. SOWA, and RCRA are perfom,ed in accordance to NE LAC protocols Pertinent sampling information is located on the attached COC Confidential Business Information· This report is provided for the exe-\usive use of the addressee Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose olher than for the addressee will be granted only on contact This ANALYT ICAL LABORATORIES Client: Energy Fuels Resources, Inc. LabSetID: 1903737 Project: Annual Seeps and Springs 2019 Analyte Result Lab Sample ID: MB-61799 Date Analyzed: Test Code: 200.7-DIS Date Prepared: --- Calcium < 1.00 Magnesium < 1.00 Potassium < 1.00 Sodium < 1.00 Vanadium < 0.00500 Lab Sample ID: MB-61800 Date Analyzed: Test Code: 200.8-DIS Date Prepared: - Arsenic < 0.000200 Beryllium < 0.000200 Cadmium < 0.0000500 Chromium < 0.000200 Cobalt < 0.000400 Copper < 0.000200 Iron < 0.0100 Lead < 0.000200 Manganese < 0.000200 Molybdenum < 0.000200 Selenium < 0.000200 Thallium < 0.000200 Tin < 0.000400 Uranium < 0.000200 Lab Sample ID: MB-FILTER-61769 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Arsenic < 0.00200 Cadmium < 0.000500 Chromium < 0.00200 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801 ) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 04/10/2019 131 lh 04/05/2019 1023h - mg/L E200 7 0.0937 1.00 mg/L E200.7 0.0439 1.00 mg/L E200 7 0.134 1.00 mg/L E200.7 0.187 1.00 mg/L E200.7 0.00138 0.00500 04/08/2019 1218h 04/05/2019 1023h mg/L E200.8 0.0000298 0.000200 mg/L E200.8 0.0000198 0.000200 mg/L E200.8 0.00000858 0.0000500 mg/L E200 8 0.000191 0.000200 mg/L E200.8 0.0000300 0.000400 mg/L E200.8 0.000282 0.000200 mg/L E200.8 0.00496 0.0100 mg/L E200.8 0.0000448 0.000200 mg/L E200.8 0.000108 0.000200 mg/L E200.8 0.0000652 0.000200 mg/L E200.8 0.0000574 0.000200 mg/L E200.8 0.0000154 0.000200 mg/L E200.8 0.000116 0.000400 mg/L E200.8 0.0000176 0.000200 04/08/2019 124 7h 04/05/2019 I 023h mg/L E200.8 0.000298 0.00200 mg/L E200.8 0.0000858 0.000500 mg/L E200 8 0.00191 0.00200 Tanner Holliday ME MBLK Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPD Amt %RPO Limit Qual Report Date: 4/11/2019 Page 11 of 26 analyses applicable to the CWA. SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling infom,ation is located on the attached COC Confidential Business lnfonnation: This report is provided for the e:'<clusive use of the addressee Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be ,grnnted only on contact This American West AN,6.LYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. LabSetID: 1903737 Project: Annual Seeps and Springs 2019 Analyte Result Lab Sample ID: MB-FIL TER-61769 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Cobalt < 0.00400 Copper < 0.00200 Manganese 0.00538 Molybdenum < 0.00200 Selenium < 0.00200 Tin < 0.00400 Lab Sample ID: MB-61800 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Nickel < 0.00200 Silver < 0.00200 Zinc < 0.00600 Lab Sample ID: MB-FILTER-61769 Date Analyzed: Test Code: 200.8-DIS Date Prepared: - Beryllium < 0.000200 Lead < 0.000200 Nickel < 0.000200 Silver < 0,000200 Thallium < 0.000200 Uranium < 0.000200 Zinc 0.000800 Lab Sample ID: MB-FILTER-61769 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Iron < 0.100 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: ( 888) 263-8686, fax: ( 801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY. REPQRT Units Method 04/08/2019 124 7h 04/05/2019 1023h mg/L E200.8 mg/L E200.8 mg/L E200,8 mg/L E200.8 mg/L E200.8 mg/L E200.8 04/09/2019 1722h 04/05/2019 1023h mg/L E200 8 mg/L E200.8 mg/L E200.8 -04/09/2019 1744h 04/05/2019 I 023h mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200.8 mg/L E200.8 04/10/2019 1533h 04/05/2019 1023h mg/L E200.8 MDL 0.000300 0.00282 0.00108 0.000652 0.000574 0.00116 0.00148 0.000232 0.00418 0.0000198 0.0000448 0.000148 0.0000232 0.0000154 0.0000176 0.000418 0.0496 Reporting Limit 0.00400 0.00200 0.00200 0.00200 0.00200 0.00400 Contact: Dept: QC Type: Amount Spiked ------ 0.00200 0.00200 0.00600 0.000200 0.000200 0.000200 0.000200 0.000200 0.000200 0.000600 0.100 Tanner Holliday ME MBLK Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual 8 Bt Report Date: 4/11/2019 Page 12 of26 cmalyses applicable to the CWA. SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling infom1atio11 is located on the attached COC Confidential Business lnfom1ation: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of tr ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL Client: Energy Fuels Resources, Inc. Lab Set ID: 1903737 Project: Annual Seeps and Springs 2019 Analyte Result Lab Sample ID: MB-61789 Date Analyzed: Test Code: HG-DW-DIS-245.1 ___ _ __ Date Prepared: Mercury < 0.0000900 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 04/10/2019 822h 04/04/2019 1830h -- mg/L E245.l 0.0000396 0.0000900 Tanner Holliday ME MBLK Spike Ref. Amount %REC Limits t -Analyte(s) were observed above the reporting limit in the jilter blank. The filter blank was acceptable, as any associated samples do not have results above the reporting limit!PQL. B -The filter blank was acceptable, as the method blank result is less than I 0% of the lowest reported sample concentration. Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual Report Date: 4/11/2019 Page 13 of26 analyses applicable to the CWA. SOWA, and RCRA are perfom1ed in accordance to NELAC protocols Pertinent sampling infom1ation is located on the attached COC Confidential Business Information: This repon is provided for the exclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement_ promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686. fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West QC SUMMARY REPORT ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday LabSetID: 1903737 Dept: ME Project: Annual Seeps and Springs 2019 QC Type: MS --- Reporting Amount Spike Ref. RPDRef. RPO Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 1903737-00IEMS Date Analyzed: 04/10/2019 1318h Test Code: 200.7-DIS Date Prepared: 04/05/2019 I 023h --- Calcium 194 mg/L E200.7 0.937 10.0 10.00 185 85.4 70 -130 Magnesium 53.6 mg/L E200,7 0.439 10.0 10.00 43.7 99.7 70 -130 Sodium 162 mg/L E200,7 1.87 10.0 10.00 152 103 70 -130 Lab Sample ID: 1903737-00lEMS Date Analyzed: 04/10/2019 1336h Test Code: 200.7-DIS Date Prepared: 04/05/2019 1023h ---- Potassium 15.5 mg/L E200.7 0.134 1.00 10.00 3.99 115 70 -130 Vanadium 0.213 mg/L E200.7 0.00138 0.00500 0.2000 0 107 70 -130 Lab Sample ID: 1903737-00lEMS Date Analyzed: 04/08/2019 1234h Test Code: 200.8-DIS Date Prepared: 04/05/2019 I 023h -- Arsenic 0.208 mg/L E200.8 0.000298 0.00200 0.2000 0.00262 103 75 -125 Cadmium 0.191 mg/L E200 8 0.0000858 0.000500 0.2000 0.0000868 95.5 75 -125 Chromium 0.196 mg/L E200 8 0.00191 0.00200 0.2000 0 97.8 75 -125 Cobalt 0.192 mg/L E200.8 0.000300 0.00400 0.2000 0.00128 95 .3 75 -125 Copper 0.192 mg/L E200.8 0.00282 0.00200 0.2000 0 95.8 75 -125 Manganese 0.711 mg/L E200.8 0.00108 0.00200 0.2000 0.528 91.6 75 -125 Molybdenum 0.201 mg/L E200.8 0.000652 0.00200 0.2000 0.003 98.9 75 -125 Selenium 0.200 mg/L E200.8 0.000574 0.00200 0.2000 0.000832 99.5 75 -125 Tin 0.986 mg/L E200,8 0.00116 0.00400 1.000 0 98.6 75 -125 Lab Sample ID: 1903737-00lEMS Date Analyzed: 04/09/2019173lh Test Code: 200.8-DIS Date Prepared: 04/05/2019 I 023h Beryllium 0.200 mg/L E200.8 0.000198 0.00200 0.2000 0 100 75 -125 Lead 0.187 mg/L E200 8 0.000448 0.00200 0.2000 0 93 .5 75 -125 Nickel 0.190 mg/L E200 8 0.00148 0.00200 0.2000 0 95.0 75 -125 Silver 0.189 mg/L E200 8 0.000232 0.00200 0.2000 0.000388 94.2 75 -125 Thallium 0.183 mg/L E200 8 0.000154 0.00200 0.2000 0 91.4 75 -125 Report Date: 4/11/2019 Page 14 of26 analyses applicable to the CWA. SOWA, and RCRA are perfom1ed in accordance to NELAC protocols Pertinent sampling infom1ation is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any pu1'pose other than for the addressee ,-vill be granted only on contact This ANALYTICAL Client: Energy Fuels Resources, Inc. Lab Set ID: 1903737 Project: Annual Seeps and Springs 2019 Analyte Result Lab Sample ID: 1903737-00lEMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Uranium 0.202 Zinc 0.977 Lab Sample ID: 1903737-00IEMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Iron 2.25 Lab Sample ID: 1903737-00lEMS Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury 0.00364 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _Q_C SUMMARY REPORT Contact: Dept: Tanner Holliday ME QC Type: MS Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 04/09/2019 1731h 04/05/2019 I 023h -- mg/L E200.8 0.000176 0.00200 0.2000 0.00491 98.5 mg/L E200.8 0.00418 0.00600 1.000 0 97.7 04/10/2019 1526h 04/05/2019 I 023h ------ mg/L E200.8 0.0992 0.200 1.000 1.2 105 04/10/2019 832h 04/04/2019 1830h -- mg/L E245.I 0.0000396 0.0000900 0.003330 0 109 -- Limits 75 -125 75 -125 75 -125 - 85 -115 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit ------ Qual Report Date: 4/11/2019 Page 15 of26 analyses applicable to the CWA. SOWA, and RCRA are perfom1ed in accordance to NE LAC protocols Pertinent samphng infom1ation is located on the attached COC. Confidential Business lnfom,ation: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tr ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West QC SUMMARY REPORT ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 1903737 Dept: ME Project: Annual Seeps and Springs 2019 QC Type: MSD --- Reporting Amount Spike Ref. RPO Ref. RPO Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 1903737-00IEMSD Date Analyzed: 04/10/2019 1320h Test Code: 200.7-DIS Date Prepared: 04/05/2019 1023h -- Calcium 198 mg/L E200,7 0.937 10.0 10.00 185 123 70 -130 194 1.93 20 Magnesium 55.3 mg/L E200,7 0.439 10.0 10.00 43.7 116 70 -130 53.6 3.06 20 Sodium 165 mg/L E200,7 1.87 10.0 10.00 152 134 70 -130 162 1.91 20 Lab Sample ID: 1903737-00IEMSD Date Analyzed: 04/10/2019 1338h Test Code: 200.7-DIS Date Prepared: 04/05/2019 1023h --- Potassium 15.3 mg/L E200 7 0.134 1.00 10.00 3.99 113 70 -130 15.5 1.42 20 Vanadium 0.211 mg/L E200.7 0.00138 0.00500 0.2000 0 106 70 -130 0.213 1.06 20 -Lab Sample ID: 1903737-00IEMSD Date Analyzed: 04/08/2019 1237h Test Code: 200.8-DIS Date Prepared: 04/05/2019 1023h ---------- Arsenic 0.209 mg/L E200.8 0.000298 0.00200 0.2000 0.00262 103 75 -125 0.208 0.495 20 Cadmium 0.188 mg/L E200 8 0.0000858 0.000500 0.2000 0.0000868 94.2 75 -125 0.191 1.46 20 Chromium 0.192 mg/L E200.8 0.00191 0.00200 0.2000 0 96.0 75 -125 0.196 1.91 20 Cobalt 0.189 mg/L E200,8 0.000300 0.00400 0.2000 0.00128 93 .6 75 -125 0.192 1.77 20 Copper 0.190 mg/L E200.8 0.00282 0.00200 0.2000 0 94.8 75 -125 0.192 1.02 20 Manganese 0.702 mg/L E200.8 0.00108 0.00200 0.2000 0.528 87.l 75 -125 0.711 1.28 20 Molybdenum 0.200 mg/L E200.8 0.000652 0.00200 0.2000 0.003 98.3 75 -125 0.201 0.529 20 Selenium 0.199 mg/L E200.8 0.000574 0.00200 0.2000 0.000832 99.0 75 -125 0.2 0.451 20 Tin 0.988 mg/L E200.8 0.00116 0.00400 1.000 0 98.8 75 -125 0.986 0.166 20 Lab Sample ID: 1903737-00IEMSD Date Analyzed: 04/09/2019 1734h Test Code: 200.8-DIS Date Prepared: 04/05/20[9 1023h Beryllium 0.199 mg/L E200.8 0.000198 0.00200 0.2000 0 99.4 75 -125 0.2 0.823 20 Lead 0.182 mg/L E200.8 0.000448 0.00200 0.2000 0 90.9 75 -125 0.187 2.81 20 Nickel 0.187 mg/L E200.8 0.00148 0.00200 0.2000 0 93.7 75 -125 0.19 1.31 20 Silver 0.189 mg/L E200 8 0.000232 0.00200 0.2000 0.000388 94.l 75 -125 0.189 0.0912 20 Thallium 0.177 mg/L E200 8 0.000154 0.00200 0.2000 0 88.6 75 -125 0.183 3.14 20 Report Date: 4/11/2019 Page 16 of26 analyses applicable to the CWA, SOWA, and RCRA are perfom1ed in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tJ- ne of this company or any member of its stafl: or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1903737 Project: Annual Seeps and Springs 2019 Analyte Result Lab Sample ID: 1903737-00lEMSD Date Analyzed: Test Code: 200.8-DIS Date Prepared: ----- Uranium 0.196 Zinc 0.984 Lab Sample ID: 1903737-00IEMSD Date Analyzed: Test Code: 200.8-DIS Date Prepared: Iron 2.22 Lab Sample ID: 1903737-00lEMSD Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury 0.00374 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Units Method 04/09/2019 1734h 04/05/2019 1023h mg/L E200.8 mg/L E200.8 04/10/2019 1530h 04/05/2019 1023h mg/L E200.8 04/10/2019 834h 04/04/2019 1830h mg/L E245.1 MDL 0.000176 0.00418 0.0992 0.0000396 Contact: Dept: QC Type: Reporting Amount Limit Spiked 0.00200 0.2000 0.00600 1.000 0.200 1.000 0.0000900 0.003330 Tanner Holliday ME MSD Spike Ref. Amount %REC 0.00491 95.5 0 98.4 1.2 102 0 112 2 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD. Limits 75 -125 75 -125 75 -125 85 -115 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. Amt %RPO --- 0.202 3.04 0.977 0.741 2.25 1.35 0.00364 2.67 RPD Limit 20 20 20 20 Qual Report Date: 4/11/2019 Page 17 of26 analyses applicable to the CWA, SOWA, and RCRA are performed in accordance to NE LAC protocols Pertinent sampling infonnat1011 is located on the attached COC Confidential Business Information: TI1is report is provided for the exclusive use of the addressee Privileges of subsequent use of tt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be ,bTfanted only on contact This ANALYTICAL Client: Energy Fuels Resources, Inc. Lab Set ID: 1903737 Project: Annual Seeps and Springs 2019 Analyte Result Lab Sample ID: 1903737-00ICDUP Date Analyzed: Test Code: TDS-W-2540C Total Dissolved Solids 1,110 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday WC DUP Spike Ref. Amount %REC 03/29/2019 1145h ---- mg/L SM2540C 16.0 20.0 Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit 1110 0.360 5 Qual Report Date: 4/11/2019 Page 18 of26 analyses applicable to the CWA. SOWA, and RCRA are perfom1ed in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC Confidential Business lnfom1ation: This report is provided for the exclusive use of the addressee Privlleges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1903737 Project: Annual Seeps and Springs 2019 Analyte Result Lab Sample ID: LCS-Rl24526 Date Analyzed: Test Code: 300.0-W Chloride 4.74 Fluoride 4.97 Sulfate 5.11 Lab Sample ID: LCS-Rl24168 Date Analyzed: Test Code: ALK-W-23208-LL Alkalinity (as CaC03) 250 Lab Sample ID: LCS-61874 Date Analyzed: Test Code: NH3-W-350. l Date Prepared: ----- Ammonia (as N) 10.8 Lab Sample ID: LCS-Rl24079 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.03 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 04/10/2019 1943h -- mg/L E300.0 0.0386 0.100 5.000 mg/L E300.0 0.0240 0.100 5.000 mg/L E300.0 0.0557 0.750 5.000 04/02/2019 749h mg/L SM2320B 0.781 1.00 250.0 04/09/2019 1646h 04/09/2019 123 5h - mg/L E350,1 0.0492 0.0500 10.00 03/29/2019 1312h --· -- mg/L E353.2 0.00363 0.0100 1.000 Tanner Holliday WC LCS Spike Ref. Amount %REC 0 94.7 0 99.3 0 102 0 100 0 108 0 103 Lab Sample ID: LCS-RI24148 Date Analyzed: 03/29/2019 1145h Test Code: TDS-W-2540C Total Dissolved Solids 180 mg/L SM2540C 8.00 10.0 205.0 0 87.8 Limits 90 -110 90 -110 90 -110 90 -110 90 -110 90 -110 80 -120 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 4/11/2019 Page 19 of 26 analyses applicable to the CWA. SOWA, and RCRA are perfom1ed in accordance to N ELAC protocols Pertinent sampling information is located on the attached COC Confidential Business Information: This repon is provided for the exclusive use of the addressee Privileges of subsequent use of ti· ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process, or in connection with the re-publication of this report for any pull)ose other than for the addressee \Vill be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1903737 Project: Arumal Seeps and Springs 2019 Analyte Result Lab Sample ID: MB-Rl24526 Date Analyzed: Test Code: 300.0-W Chloride < 0.100 Fluoride <0.100 Sulfate < 0.750 Lab Sample ID: MB-Rl24168 Date Analyzed: Test Code: ALK-W-2320B-LL Bicarbonate (as CaC03) < 1.00 Carbonate (as CaC03) < 1.00 Lab Sample ID: MB-61874 Date Analyzed: Test Code: NH3-W-350. l Date Prepared: Ammonia (as N) < 0.0500 Lab Sample ID: MB-R124079 Date Analyzed: Test Code: N02/N03-W-353.2 ------ Nitrate/Nitrite (as N) < 0.0100 Lab Sample ID: MB-Rl24148 Date Analyzed: Test Code: TDS-W-2540C Total Dissolved Solids < 10.0 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 04/10/2019 1926h - mg.IL E300.0 0.0386 0.100 mg/L E300.0 0.0240 0.100 mg/L E300.0 0.0557 0.750 04/02/2019 749h mg.IL SM2320B 0.781 1.00 mg.IL SM2320B 0.781 1.00 04/09/2019 1645h 04/09/2019 123 5h - mg/L E350,l 0.0492 0.0500 03/29/2019 1310h mg.IL E353.2 0.00363 0.0100 03/29/2019 1145h mg/L SM2540C 8.00 10.0 Tanner Holliday WC MBLK Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPO Limit Qual Report Date: 4/11/2019 Page 20 of26 analyses applicable to the CWA. SOWA, and RCRA are perfom1ed in accordance to NELAC protocols Pertinent samphng informat10n is located on the attached CO(' Confidential Busines~ lnfom1ation: This report is provided for the exclusive me of the addressee Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of thls report in connection with the adve1tisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This Client: Energy Fuels Resources, Inc. Lab Set ID: 1903737 Project: Arumal Seeps and Springs 2019 Analyte Result Lab Sample ID: 1903737-00lBMS Date Analyzed: Test Code: 300.0-W Chloride 502 Fluoride 480 Sulfate 947 Lab Sample ID: 1903737-00lBMS Date Analyzed: Test Code: ALK-W-23208-LL Alkalinity (as CaC03) 1,450 Lab Sample ID: 1903737-00lDMS Date Analyzed: Test Code: NH3-W-350.I Date Prepared: Ammonia (as N) 10.8 Lab Sample ID: 1903737-00lDMS Date Analyzed: Test Code: N02/N03-W-353.2 ---- Nitrate/Nitrite (as N) 11.0 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 04/10/2019 2305h --- mg/L E300.0 3.86 10.0 500.0 mg/L E300.0 2.40 10.0 500.0 mg/L E300.0 5.57 75.0 500.0 04/02/2019 749h ~ mg/L SM2320B 0.781 1.00 1,000 04/09/2019 1650h 04/09/2019 1235h - mg/L E350.I 0.0492 0.0500 10.00 03/29/2019 1314h ---- mg/L E353.2 0.0363 0.100 10.00 Tanner Holliday WC MS Spike Ref. Amount %REC 41.6 92.1 0 96.1 436 102 450 100 - 0 108 0 110 § -QC limits are set with an accuracy of two significant figures, therefore the recovery rounds to an acceptable value within the control limits. Limits 90 -110 90 -110 90 -110 80 -120 90-110 90 -110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual § Report Date: 4/11 /2019 Page 21 of26 analyses applicable to the CWA. SOWA, and RCRA are perfom1ed in acco,d:mc.e to NELAC protocols Pertinent sampling infom1ation is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use oft~ TIC of this company or any member of its staft: or reproduction of this report in connection with the adve1'tisement promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer ANALYTICAL LABORATORIES _QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 1903737 Dept: WC Project: Annual Seeps and Springs 2019 QC Type: MSD ---- Reporting Amount Spike Ref. RPO Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 1903737-00lBMSD Date Analyzed: 04/10/2019 2322h Test Code: 300.0-W --- Chloride 509 mg/L E300.0 3.86 10.0 500.0 41.6 93.5 90 -110 502 1.36 20 Fluoride 486 mg/L E300.0 2.40 10.0 500.0 0 97.2 90 -110 480 1.16 20 Sulfate 945 mg/L E300,0 5.57 75.0 500.0 436 102 90 -110 947 0.234 20 Lab Sample ID: 1903737-00lBMSO Date Analyzed: 04/02/2019 749h Test Code: ALK-W-2320B-LL -- Alkalinity (as CaC03) 1,460 mg/L SM2320B 0.781 1.00 1,000 450 IOI 80 -120 1450 0.275 10 Lab Sample ID: 1903737-00IDMSO Date Analyzed: 04/09/2019 1651 h Test Code: NH3-W-350.1 Date Prepared: 04/09/2019 1235h ------ Ammonia (as N) 10.7 mg/L E350.1 0.0492 0.0500 10.00 0 107 90 -110 10.8 0.929 10 Lab Sample ID: 1903737-00IDMSO Date Analyzed: 03/29/2019 1316h Test Code: N02/N03-W-353.2 ------- Nitrate/Nitrite (as N) 10.6 mg/L E353.2 0.0363 0.100 10.00 0 106 90 -110 11 3.70 10 Report Date: 4/11/2019 Page 22 of26 analyses applicable to the CWA. SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling infom1at1on is located on the attached COC Confidential Business Information: This report is provided for the e;,,;clusive use of the addressee, Privileges of subsequent use of tl- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1903737 Project: Annual Seeps and Springs 2019 Analyte Result Lab Sample ID: LCS VOC-2 032919A Date Analyzed: Test Code: 8260-W-DENIOO -- Benzene 20.7 Chlorofonn 19.8 Methylene chloride 20.0 Naphthalene 16.6 Tetrahydrofuran 16.1 Toluene 20.8 Xylenes, Total 66.9 Surr: l ,2-Dichloroethane-d4 46.6 Surr: 4-Bromofluorobenzene 49.5 Surr: Dibromofluoromethane 50.2 Surr: Toluene-dB 51.8 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA LCS Spike Ref. Amount %REC 03/29/2019 743h µg/L SW8260C 0.147 1.00 20.00 0 104 µg/L SW8260C 0.166 1.00 20.00 0 99.2 µg/L SW8260C 0.448 1.00 20.00 0 99.8 µg/L SW8260C 0.704 1.00 20.00 0 83.3 µg/L SW8260C 0.436 1.00 20.00 0 80.4 µg/L SW8260C 0.177 1.00 20.00 0 104 µg/L SW8260C 1.00 60.00 0 111 µg/L SW8260C 50.00 93.3 µg/L SW8260C 50.00 99.0 µg/L SW8260C 50.00 100 µg/L SW8260C 50.00 104 Limits 82 -132 85 -124 65 -154 63 -129 59 -125 69 -129 66 -124 80 -136 85 -121 78 -132 81 -123 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 4/11/2019 Page 23 of26 analyses applicable to the CWA. SOWA, and RCRA are perfonned m accordance to NELAC protocols Pertinent sampling infom1ation is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1903737 Project: Annual Seeps and Springs 2019 Analyte Result Lab Sample ID: MB VOC-2 032919A Date Analyzed: Test Code: 8260-W-DENJOO 2-Butanone <20.0 Acetone <20.0 Benzene < 1.00 Carbon tetrachloride < 1.00 Chloroform < 1.00 Chloromethane < 1.00 Methylene chloride < 1.00 Naphthalene < 1.00 Tetrahydrofuran < 1.00 Toluene < 1.00 Xylenes, Total < 1.00 Surr: l ,2-Dichloroethane-d4 47.9 Surr: 4-Bromofluorobenzene 53.4 Surr: Dibromofluoromethane 49.0 Surr: Toluene-d8 51.0 --- Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA MBLK Spike Ref. Amount %REC 03/29/2019 823h µg/L SW8260C 1.31 20.0 µg/L SW8260C 2.87 20.0 µg/L SW8260C 0.147 1.00 µg/L SW8260C 0.262 1.00 µg/L SW8260C 0.166 1.00 µg/L SW8260C 0.832 1.00 µg/L SW8260C 0.448 1.00 µg/L SW8260C 0.704 1.00 µg/L SW8260C 0.436 1.00 µg/L SW8260C 0.177 1.00 µg/L SW8260C 1.00 µg/L SW8260C 50.00 95.9 µg/L SW8260C 50.00 107 µg/L SW8260C 50.00 98.0 µg/L SW8260C 50.00 102 Limits 80 -136 85 • 121 78 • 132 81 -123 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPO Limit Qual Report Date: 4/11/2019 Page 24 of26 analyses applicable to the CWA. SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling infom1ation is located on the attached COC Confidential Business lnfom1ation: TI1is report is provlded for the exclusive use of the addressee Privileges of 5ubsequent use oft~ ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1903737 Project: Annual Seeps and Springs 2019 Analyte Result Lab Sample ID: 1903737-00lAMS Date Analyzed: Test Code: 8260-W-DENIOO -- Benzene 21.3 Chloroform 20.5 Methylene chloride 20.5 Naphthalene 16.4 Tetrahydrofuran I 7.8 Toluene 21.5 Xylenes, Total 68.8 Surr: I ,2-Dichloroethane-d4 47.8 Surr: 4-Bromofluorobenzene 50.2 Surr: Dibromofluoromethane 51.5 Surr: Toluene-d8 51.l Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA MS Spike Ref. Amount %REC 03/29/2019 1319h ~ -- µg/L SW8260C 0.147 1.00 20.00 0 107 µg/L SW8260C 0.166 1.00 20.00 0 103 µg/L SW8260C 0.448 1.00 20.00 0 103 µg/L SW8260C 0.704 1.00 20.00 0 81.8 µg/L SW8260C 0.436 100 20.00 0 89.2 µg/L SW8260C 0.177 1.00 20.00 0 108 µg/L SW8260C 1.00 60.00 0 115 µg/L SW8260C 50.00 95.7 µg/L SW8260C 50.00 100 µg/L SW8260C 50.00 103 µg/L SW8260C 50.00 102 Limits 66 -145 50 -146 30 -192 41 -131 43 -146 18 -192 42 -167 72-151 80 -152 72 -135 80-124 ---- Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual ReportDate: 4/11/2019 Page25of26 analyses applicable to the CWA. SOWA, and RCRA are perfom1ed in accordance to NELAC protocols Pertinent sampling information is located on the attached CO(' Confidential Business lnfom1ation: This report is provided for the exclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its stat{ or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. LabSetID: 1903737 Project: Annual Seeps and Springs 2019 Analyte Result Lab Sample ID: 1903737-00IAMSD Date Analyzed: Test Code: 8260-W-DENIOO Benzene 20.8 Chloroform 20.0 Methylene chloride 20.0 Naphthalene 15.9 Tetrahydrofuran 18.7 Toluene 20.8 Xylenes, Total 66.5 Surr: I ,2-Dichloroethane-d4 47.3 Surr: 4-Bromofluorobenzene 49.5 Surr: Dibromofluoromethane 50.4 Surr: Toluene-d8 50.5 Units 3440 South 700 West Salt Lake City, UT 84 I 19 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT_ Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA MSD Spike Ref. Amount %REC 03/29/2019 1339h ---- µg/L SW8260C 0.147 1.00 20.00 0 104 µg/L SW8260C 0.166 1.00 20.00 0 100 µg/L SW8260C 0.448 1.00 20.00 0 100 µg/L SW826DC 0.704 1.00 20.00 0 79.4 µg/L SW8260C 0.436 1.00 20.00 0 93.5 µg/L SW8260C 0.177 1.00 20.00 0 104 µg/L SW8260C 1.00 60.00 0 111 µg/L SW8260C 50.00 94.6 µg/L SW8260C 50.00 99.0 µg/L SW826DC 50.00 101 µg/L SW826DC 50.00 IOI Limits 66 -145 50 -146 30 -192 41 -131 43 -146 18 -192 42 -167 72 -151 80 -152 72 -135 80 -124 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit 21.3 2.42 25 20.5 2.52 25 20.5 2.32 25 16.4 3.10 25 17.8 4.71 25 21.5 3.26 25 68.8 3.36 25 Qual Report Date: 4/11 /2019 Page 26 of26 analyses applicable to the CWA. SOWA, and RCRA are perfonned in accordance to NELAC protocols Pertinent samphng infomiation is located on the attached COC Confidential Business lnfonnation: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with there-publication of this report for any purpose other than for the addressee will be granted only on contact This American West Analytical Laboratories WORK ORDER Summary Client: Client ID: Project: Comments: Sample ID 1903737-00lA 1903737-00lB 1903737-00lC 1903737-00lD 1903737-00IE 1903737-002A Energy Fuels Resources, Inc. ENE300 Contact: Annual Seeps and Springs 2019 QC Level: QC 3 (no chromatograms). EDD-Denison. CC KWeinel@energyfuels.com.; Client Sample ID Collected Date Received Date Westwater Seep 3/27/2019 0930h 3/29/2019 1000h Trip Blank 3/27/2019 0930h 3/29/2019 1 OOOh Tanner Holliday III Rpt Emailed: WorkOrder: 1903737 Due Date: 4/12/2019 WO Type: Project UL Denison Page 1 of 1 ~ Test Code Matrix Sel Storage 8260-W-DENlOO Aqueous VOCFridge 3 Test Group: 8260-W-DENJOO; # of Analytes: 11 I# ojSurr: 4 300.0-W df-wc 3 SEL Analytes: CL F S04 ALK-W-2320B-LL df-wc 2 SEL Analytes: ALKB ALKC TDS-W-2540C df-tds 1 SEL Analytes: TDS NHJ-W-350.1 df -no2/no3 & nh3 1 SEL Analytes: NH3N NH3-W-PR df -no2/no3 & nh3 N02/N03-W-353.2 df -no2/no3 & nh3 1 SEL Analytes: N03N02N 200.7-DIS df-met 5 SEL Analytes: CA MG K NA V 200. 7-DIS-PR df-met 200.8-DIS df-met 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NJ SE AG TLSNUZN 200.8-DIS-PR df-met HG-DW-DIS-245.1 df-met 1 SEL Analytes: HG HG-DW-DIS-PR df-met IONBALANCE df-met 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 8260-W-DENlOO Aqueous VOCFridge 3 Test Group_: 8260-W-DENJOO; # of Analytes: 11 I# ojSurr: 4 Printed: 03/29/19 11:14 LABORATORY CHECK: %M O RT D CN O TAT O QC O LUO 0 HOK ___ HOK __ _ HOK___ COG Emailed:.._ ___ _ 3 : 5 6 i i 8 9 10 I 12 : Address: Contact: Phone#: Email: Project Name: Project#: PO#: Sampler Name: Westwater Seep Trip Blank American West Analytical Laboratories 463 W. 3600 S. Salt Lake City, UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 6425 S. Hwy. 191 Blanding, UT 84511 Tanner Holliday (435) 678-2221 Cell#: gpalmel@energyfuels.com; KWeiDel@energyfuels.com; thollidaEne!lllfuels.com Annual Seeps and Springs 2019 Tanner Holliday Date Sample ID: Sampled 1 3/27/2019 3/27/2019 Rollnq\.ts!)ed oy: ~,1/11')1,.-~~f Dale! Sl!lnalln 3128120H u Timre PmtNilme: TaMer Holffri>v ,,ao Re!lrqtdshed by. Date; --[Tm,e: PrtnlN"""" Relinquished by: Date: '""'nalu-e Time: Print Name: Relinquished by: Date: L~nnalU'e Time: PrintN.arne: Time Sampled 930 930 Received by: Sia nature Prin!Name: Received by: Slanature Print Name: Recehled by: Sionature PrlnlName: ReceiVe<lby: Slanalure ., PriatName·- I CHAIN OF CUSTODY 190~?61 All analysis will be comlucted using NELAP accre<lted methods aml all data wlll be reported using AWAL's standard analyte lists and reporting limilS {PQL) ooless specifically requested olherwise oo this Chain or Custody and/or attac!led docm,entatlon. AWAL Lab Sample Set# Page 1 of 1 QC Level: I Tum Around Time: Unless other arrangements have been made, 1°"11' I -z-\ \ 9 I signed reports will be emailed by 5:00 pm on 3 Standard the day they are due. X Include EDD: Laboratory Use Only 0 LOCUS UPLOAD ISam~~w~~ ~ ::;: al u EXCEL on bD X Field Filtered For: -... tt: ::;: Dissolved Metals 1 ~ hand <ID!lVe<ed .... i:::· v:i ::;: :i 2 Amblenlo~ 'I-C"l .0 ci ~ p.. z For Compliance With: a TemperallJre Or3 c:; ci j 0 NELAP 'C 0 0 RCRA o' C"l ;:i ::,.· D CWA 4 Received Broken/leaking C) ~ 0 c:; u :i' 0 SOWA {Improperly Seal~ -... "l a 0 0 El.AP / A2LA y N .... ... ~ i:::· c:i tl. u 0 a (/J 0 NLLAP c;-lJ) a C"l .. .... 0 Non-Compliance 5 0""Y Preserved "l a "l ] u ~:: l;j ... 1/) tl. ,d 0 Other: . y N 0 :::t. 4D i D' ~ !2.. \J D' ,e :.: u cu a Checked at bench )( a """ a "' Cl IO y N C: ·c: (') 0 0 ;Ji Cl '1::1 .; .; ; C'l ~ iu 0 1/) fll a cu C!l (/J ~ Known Hazards 6 Received Within ::;; Ii!; :::t. tl. .:: .; 0 " ...... 0 ...... 0 rti i ~ .. g~nmes u C. 8 (') fll = .. < u & 0 E = s ~ .!l II 0 N ., 0 Samele Comments "" en Ii!; I!'; u 1:1 ... > 7 w X ; .;;: X" X X X X X X ft \ ' \">'.:v~ 3 w X ~w:,-J""' . . N 2&er, on Outer P y N I 3 Present on Sample 0 Y N NA ·" 4 Unbroken on sample ·A Y N , NA - Discrepancies Between Sample y N Labels and COC Recc<~ Dale: Special Instructions: lme: Sample containers for metals were field filtered. See the Date: Analytical Scope of Work for Reporting Limits and voe analyte Time: list. Dale: Time: -A . )o AL o'.f\~ ~~>,. 1AJ D~lz_ql \9 --:)(?'->-j{\\tgz_ -g.('( 1\.) .. 'C"°I rnmel ff\ :'co Analysis Ammonia COD Cyanide Metals N02/N03 O&G Phenols Sulfide TKN TP04 CrVI+ Procedure: Frequency: Preservation Check Sheet s amo le Set E Preservative f-OOl pH<2 H2S04 "o~ pH <2H2S04 pH>12NaOH pH<2HN03 ,'P4 pH<2H2S04 ·, R,.J pH<2HCL pH<2 H2S04 pH>9NaOH, Zn Acetate pH<2H2S04 pl-1<2 H2S04 pH>9 (NH4)iSQ4 Pour a small amount of sample in the sample lid Pour sample from lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid doH l) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client ifrequested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + • # • The sample required additional preservative upon receipt. The sample was received unpreserved. The sample was received unpreserved and therefore preserved upon receipt. The sample pH was unadjustable to a pH < 2 due to the sample matrix. The sample pH was unadjustable to a pH> __ due to the sample matrix interference . Lab Set ID: pH Lot#: \ qo3J~] 59,ID l!;l 4 • Labo rato ries LLc a member of The GEL Group INC PO Box 3'0712 Cria~ e,wn SC 29417 2040 Smg~ Road Cha~eston SC 29407 P 843.556.8171 P 84'.l.766.1178 April 26, 2019 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: Analytical for Annual Seeps and Spring 2019 Work Order: 475027 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on April 01 , 2019. This revised data report has been prepared and reviewed in accordance with GEL's standard operating procedures. This package has been revised to show correct method. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DW16138 Enclosures Sincerely, ~~~ Juli.e Robin on Project Manager mt 1111111 1m~ 11111111 !' 1111111111 gel.co m Energy Fuels Resources (USA), Inc. Analytical for SDG: 475027 This package has been revised to show correct method. April 26, 2019 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 475027 Sample receipt: The sample arrived at GEL Laboratories LLC, Charleston, South Carolina on April 01, 2019 for analysis. The sample was delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following sample: Laboratory ID Client ID 475027001 Westwater Seep Case Narrative: Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. ~~S;- Julie Robinson Project Manager Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: _G_e_l _La_b_o_ra_t_o_rie_s _________ Contact: Tanner Holliday 2040 Savage Road Ph: 435 678 4115 Charleston, SC 29407 tholliday@enerqyfuels.com Chain of Custody/Sampling Analysis Request p . t ro1ec s amp ers N ame s amp ers Si 1gnature Annual Seeps and Spring L \,, 12.nJJ, . .JUl-:1. 1 2019 Tanner Holliday ,./ Time Sample ID Date Collected Collected Laboratory Analysis Requested Westwater seep 3/27/2019 930 Gross Alpha Comments: A..JJ/,fa Relinquished By:(Signature) Datemme Received By:(Signature) Daterr e ~~niJ.~-1 3/28/2019 ~ .8i{a~ 1130 Relinquished By:(Signature) V Date/Time Receive~ignature) Date/Time r.:r.:1'111 i "t)nr::1'torio" ' ' ,. ~ Ld v1\.l ,,v0 1!..'.._. Cllcqt: Received By: ZKW Carrier and Tracking Number Sus1>cctcd I-lazord Information A)Ship ed as a DOT Hazardous'/ B) Did the client designate the samples are lo be received as radioactive? C) Did the RSO classil)' the samples as radioactive? D) Did the client designate samples arc hazardons? E) Did the RSO identi fv ossiblc hazards'/ Sample Receipt Criteria Shipping containers received intact and scaled? 2 Chain of custody documents included with shi mcnt? 3 Samples requiring cold preservation within (0 5 6 deg. C)?* 4 Daily check performed and passed on IR tcmperoture gun' 5 Sample containers intact and scaled? 6 Samples requiring chemical preservation i1t proper pH? 7 Do any samples require Volatile Analysis? 8 Snm1ilcs received within holding time? 9 Sample ID's on COC match ID's on boulcs? 10 Date & time on COC match date & time on bottles? 11 Number of containers received match nu111bcr indicated on COC? 12 13 COC form is properly signed in rcllnquishcd/rccoivccl sections? Comments (Use Con1inu:,1ion Fann if needed): SAMPLE RECEIPT & REVlEW FORM SDG/AIUCOC/WorkOr er: '-/ 1 c= D~ l Date Received: FedEx Express Circ~lo: FedEx Ground e;Field Services Courier Other tc ~ -:_ •JrNct Counts > IOOcpm on samples not marked "radioactive". contact the Radiation Safety Group for funher investigation. Hnwrd Class Shipped: UN#: fUN2910, Is the Radioactive Shipment Survey Compliant? Yes_ No_ RCRA Asbestos Beryllium Other: Comments/Qualifiers (Required for Non-Conforming Items) Cude Applicable: ScoJs broken Dmm1yc<l (:Ontniucr L\lnL:in~ container 01hc.r (dll!Stlriba) Ciro!c ,\pplicoblc: Client comactcd ,nd provided COC Prcservntion Method: Wet Ice Ice Packs Dry ice •all lcmpcratures are recorded in Celsius Tcm11cr11turc De\'icc Serini II: IR3-1B Secondary Temperature Device Serial II (If Applicable): COC <r<>tcd upon r«cipt Cir-c:h,: Applicable: Sc"b brok~n DamiJgcd Cl1nlaincr Lc:1krng conrniner Other {describe) Somrtc ID'~ ond Conto1ncrs Alf<o1od: TEMP: L-/ ., L. Do liquid VOA vials conrnin ncid preservation? Yes __ No_ NA __ (lfunknown, select No) 1 re liquid VOA vials free ofhcnd~1incc? Yes_ No_ NA_ 10·~ nnd tests ~ncctcd: ID's nnd containers nffcctctl: Circle Applicable: 'o dntcs on containers No times on containers COC missing info Other (describe) Circle Af)plicnblc: No container count on COC Other (describe) Circle Applicable: 'nt relinquished Other (dw:ribc) GL-CHL-SR-001 Rev 6 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 475027 Client SDG: 475027 Annual Seeps and Spring 2019 Project Manager: Project Name: Purchase Order: Package Level: EDD Format: Julie Robinson DNMI00106 Analytical for DW16138 LEVEL3 EIM_DNMI GELID Client Sample ID Client Sample Desc. Collect Date & Time Work Order Due Date: 29-APR-19 Package Due Date: 27-APR-19 EDD Due Date: QA Due Date: tJAtitt>ate: Receive Time # of Date & Time Zone Cont. 29-APR-19 29-APR-19 30-APR-19 Lab Matrix Report Date: 26-APR-19 Work Order: 475027 Page 1 of 2 Collector: C Prelogin #: 20190486669 Project Workdef ID: 1329132 SDG Status: Closed Logged by: Fax Days to Due Date Process CofC# Prelog Lab Field Group QC QC 475027001 Westwater Seep 27-MAR-19 09:30 01-APR-19 08:55 -2 GROUND WATER 20 Client Sample ID -001 Westwater Seep Status Tests/Methods REVW GFPC, Total Alpha Radium, Liquid Product Reference Gross Alpha Fax Date PM Comments Aux Data Product: GFCTORAL Workdef ID: 1461303 In Product Group? No Group Name: Group Reference: Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Samples: 001 Parmname Check: All parmnames scheduled properly CAS# Contingent Tests Parmname Gross Radium Alpha Action Product Name Login Requirements: Requirement Description Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Client RDL or PQL & Unit Reporting Parm Included Included Custom Units Function in Sample? in QC? List? pCi/L REG y y No Samples Include? Comments Receive Codes ( GEL Laboratories LLC -Login Review Report Peer Review by:, ___________ _ Work Order (SDG#), PO# Checked? ____ _ Report Date: 26-APR-19 Work Order:475027 Page 2 of 2 C of C signed in receiver location? _____ _ List of current GEL Certifications as of 26 April 2019 State Certification Alaska 17-018 Arkansas 88-0651 CLIA 42D0904046 California 2940 Colorado SC00012 Connecticut PH-0169 DoD ELAP/ ISOl 7025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Pennit P330-15-00283,P330-15-00253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SDWA 90129 Kentucky Wastewater 90129 Louisiana NELAP 03046 (AI33904) Louisiana SDWA LA024 Maryland 270 Massachusetts M-SC012 Michigan 9976 Mississippi SC00012 Nebraska NE-OS-26-13 Nevada scooo 122019-3 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania NELAP 68-00485 Puerto Rico SC00012 S. Carolina Radiochem 10120002 South Carolina Chemistry 10120001 Tennessee TN 02934 TexasNELAP Tl04704235-19-15 UtahNELAP SC000122018-27 Vermont VT87156 Virginia NELAP 460202 Washington C780 Radiochemistry Technical Case Narrative Energy Fuels Resources (DNMI) SDG #: 475027 Product: GFPC, Total Alpha Radium, Liquid Analytical Method: EPA 903.0 Analytical Procedure: GL-RAD-A-044 REV# IO Analytical Batch: 1863376 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 475027001 1204251123 1204251124 1204251125 1204251126 1204251127 Client Sam pie Identification Westwater Seep Method Blank (MB) 47502700l(Westwater Seep) Sample Duplicate (DUP) 47502700l(Westwater Seep) Matrix Spike (MS) 47502700l(Westwater Seep) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Preparation Information Aliquot Reduced Aliquots were reduced due to limited sample volume. Miscellaneous Information Additional Comments The matrix spike and matrix spike duplicate, 1204251125 (Westwater SeepMS) and 1204251126 (Westwater SeepMSD), aliquots were reduced to conserve sample volume. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMI001 Energy Fuels Resources (USA), Inc. Client SDG: 475027 GEL Work Order: 475027 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. Review/Validation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: J~ ~ Date: 26 APR 2019 Name: Theresa Austin Title: Group Leader GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Workorder: Parmname Rad Gas Flow Suite 600 Lakewood, Colorado Ms. Kathy Weinel 475027 3atch 1863376 QC1204251124 475027001 DUP Gross Radium Alpha QC1204251127 LCS Gross Radium Alpha QCl204251123 MB Gross Radium Alpha QC1204251125 475027001 MS Gross Radium Alpha QC1204251126 475027001 MSD Gross Radium Alpha Notes: NOM u Uncertainty 887 Uncertainty Uncertainty 4450 u Uncertainty 4450 u Uncertainty Sam le 0.232 U +/-0.270 0.232 +/-0.270 0.232 +/-0.270 u Counting Uncertainty is calculated at the 68% confidence level (I-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product 0.721 +/-0.313 780 +/-10.1 0.249 +/-0.282 3780 +/-52.1 3720 +/-50.7 pCi/L NIA pCi/L pCi/L pCi/L pCi/L 1.45 A B BO C D F H K L M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Reoort Date: April 26, 2019 Page 1 of REC% Ran e Anlst -----" Date Time NIA JXC9 04/05/19 12:2 87.9 (75%-125%) 04/05/19 12:2 04/05/19 12:2 84.8 (75%-125%) 04/05/19 12:2 83.5 (0%-20%) 04/05/19 12:2 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 475027 Parmname NOM RPO% REC%_----'RC..Ca"'-nge Anlst M Matrix Related Failure NIA RPD or %Recovery limits do not apply. NI ND NJ Q R u UI UJ UL X y I\ h See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of Date Time NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPO not applicable. /\ The Relative Percent Difference (RPO) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is Jess than 5X the RL, a control limit of +I-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Tanner Holliday Energy Fuels Resources, Inc. 6425 South Hwy 191 American West Blanding, UT 84511 ANALYTICAL LABORATORIES 3440 South 700 West ;;alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail : awal@awal-labs.com web: www.awal-Jabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer TEL: ( 435) 678-2221 RE: Seeps and Springs 2019 Dear Tanner Holliday: Lab Set ID: 1906343 American West Analytical Laboratories received sample(s) on 6/13/2019 for the analyses presented in the following report. American West Analytical Laboratories (AW AL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, Wyoming, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation '1Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The ''Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Digitally signed by Jose G. J OS e G ~~c~~=Jose G. Rocha, • o=American West Analytical Laboratories, ou, RO Ch a ~:~tjose@awal-labs.com, Date: 2019.07.05 14:33:52 Approved by: -os·oo· Laboratory Director or designee Report Date: 7/5/2019 Page I of35 All annl~ ses applicable lo lhe CWA. SOWA. and RCRA me perfom,ed in accordance to NELAC p1otocols Pertinent sampling i11forrnn1ion is locnted on Lhe attached COC Confide1111al Business Information: This repor1 is prm 1ded for 1he exclusi\"e use of the ~ddressee Pri, ile~es o: sub~seq~enl ~1~e or the ~~e of this .coi~pm1~ or M) 1~mbe1 of its slaff. or reproduclio~ ~! ll1is I epo~ in ,co11~1ec1ion~ \\ill1 lhe a~, ertisemenl p~omolio.n 01 sale of :U!~ ~1odl~L or p1,ocess, ~r in ~onn;c!im1 w!lh th; r;:publicntio11 of this report SAMPLE SUMMARY Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: Seeps and Springs 2019 Lab Set ID: 1906343 Date Received: 6/13/2019 1054h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 3440 South 700 West 1906343-00 IA Entrance Seep 6/11/2019 815h Aqueous VOA by GC/MS Method ,altLakeCity,UT 84119 8260C/5030C 1906343-001B Entrance Seep 6/11/2019 815h Aqueous Anions, E300.0 1906343-001B Entrance Seep 6/11/2019 815h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level Phone: (801) 263-8686 1906343-001 C Entrance Seep 6/11/2019 815h Aqueous Total Dissolved Solids, A2540C Toll Free: (888) 263-8686 1906343-001 D Entrance Seep 6/11/2019 815h Aqueous Nitrite/Nitrate (as N), E353.2 Fax: (801) 263-8687 1906343-001D Entrance Seep 6/11/2019 815h Aqueous Ammonia, Aqueous ~-mail: awal@awal-labs.com 1906343-00 lE Entrance Seep 6/11/2019 815h Aqueous Mercury, Drinking Water Dissolved web: www.awal-labs.com 1906343-00 lE Entrance Seep 6/11/2019 815h Aqueous Ion Balance 1906343-00 lE Entrance Seep 6/11/2019 815h Aqueous ICP Metals, Dissolved 1906343-00lE Entrance Seep 6/11/2019 815h Aqueous ICPMS Metals, Dissolved Kyle F. Gross l 906343-002A Ruin Spring 6/11/2019 850h Aqueous VOA by GC/MS Method 8260C/5030C Laboratory Director 1906343-0028 Ruin Spring 6/11/2019 850h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level Jose Rocha 1906343-0028 Ruin Spring 6/11/2019 850h Aqueous Anions, E300.0 QA Officer l 906343-002C Ruin Spring 6/11/2019 850h Aqueous Total Dissolved Solids, A2540C l 906343-002D Ruin Spring 6/11/2019 850h Aqueous Nitrite/Nitrate (as N), E353.2 l 906343-002D Ruin Spring 6/11/2019 850h Aqueous Ammonia, Aqueous l 906343-002E Ruin Spring 6/11/2019 850h Aqueous Mercury, Drinking Water Dissolved l 906343-002E Ruin Spring 6/11/2019 850h Aqueous Ion Balance l 906343-002E Ruin Spring 6/11/2019 850h Aqueous ICP Metals, Dissolved l 906343-002E Ruin Spring 6/11/2019 850h Aqueous ICPMS Metals, Dissolved l 906343-003A Cottonwood Spring 6/11/2019 950h Aqueous VOA by GC/MS Method 8260C/5030C 1906343-0038 Cottonwood Spring 6/11/2019 950h Aqueous Anions, E300.0 1906343-0038 Cottonwood Spring 6/11/2019 950h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level l 906343-003C Cottonwood Spring 6/11/2019 950h Aqueous Total Dissolved Solids, A2540C l 906343-003D Cottonwood Spring 6/11/2019 950h Aqueous Nitrite/Nitrate (as N), E353.2 l 906343-003D Cottonwood Spring 6/11/2019 950h Aqueous Ammonia, Aqueous l 906343-003E Cottonwood Spring 6/11/2019 950h Aqueous Mercury, Drinking Water Dissolved l 906343-003E Cottonwood Spring 6/11/2019 950h Aqueous Ion Balance Report Date: 7/5/2019 Page 2 of35 All analyses applicnble Lo lhe CWA. SDWA and RCRA we performed in accordance Lo NELAC protocols Pertinent sampling inrormalion is located on the allnched COC Confidential Business Information: This 1epor1 is provided for lhe exclusi,-e use of the ~ddressee P1i, ile~es o.r sub~seq~ent ~1~e of the ~~e of 1his 0 cm~pan)· or ffil)" 1~mbe1 of its stnff. or re1)roductio1~ ~f this repo~ in ~011~1eclion~ \\ilh the a~, ertisement p~omolio.n 4:r sale of !"l). ~1 od~cl or p1:ocess, ~r in ~onn:_c~ion "~lh lh~ r:-publication or this report 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Client: Project: Lab Set ID: Date Received: Lab Sample ID l 906343-003E l 906343-003E 1906343-004A l 906343-004B l 906343-004B 1906343-004C l 906343-004D 1906343-004D l 906343-004E l 906343-004E 1906343-004E 1906343-004E 1906343-00SA Energy Fuels Resources, Inc. Seeps and Springs 2019 1906343 6/13/2019 1054h Client Sample ID Cottonwood Spring Cottonwood Spring Back Spring Back Spring Back Spring Back Spring Back Spring Back Spring Back Spring Back Spring Back Spring Back Spring Trip Blank Contact: Tanner Holliday Date Collected Matrix Analysis 6/11/2019 950h Aqueous ICP Metals, Dissolved 6/11/2019 950h Aqueous ICPMS Metals, Dissolved 6/11/2019 850h Aqueous VOA by GC/MS Method 8260C/5030C 6/11/2019 850h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level 6/11/2019 850h Aqueous Anions, E300.0 6/11/2019 850h Aqueous Total Dissolved Solids, A2540C 6/11/2019 850h Aqueous Nitrite/Nitrate (as N), E353.2 6/11/2019 850h Aqueous Ammonia, Aqueous 6/11/2019 850h Aqueous Ion Balance 6/11/2019 850h Aqueous ICP Metals, Dissolved 6/11/2019 850h Aqueous ICPMS Metals, Dissolved 6/11/2019 850h Aqueous Mercury, Drinking Water Dissolved 6/11/2019 815h Aqueous VOA by GC/MS Method 8260C/5030C Report Date: 7/5/2019 Page 3 of35 All nnnl)ses applicoble lo the CWA. SDWA. and RCRA ate performed in accordance to NELAC protocols Pertinent sampling i11for111ation is located on Lhe attached COC Confidential Business Information: This report is prmided for lhe exclusi\e use or the ~ddressee P1i\ ile~es o.f sub .. seq~enl ~~e of the ~?1:"e of this.co1~pa11y or M) 1~mbe1 of its stnfT, or reproducti~ ~f1his repo~ in ~on!'echon~ \\ilh the o.~, ertisemenl, p~omo1io 0 n or sale of~!~ ~rod1!cl or p1 0 ocess, ?r in ~ru1~~ion "!lh lh~ r:-publicntion of lhis 1eporl 3440 South 700 West ,alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-0-C Discrepancies: Seeps and Springs 2019 1906343 6/13/2019 6/11/2019 Intact None Holding Time and Preservation Requirements: The analysis and preparation of all samples were performed within the method holding times. All samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, DUP: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike / Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exceptions: Sample ID Analyte QC Explanation 190343-002E Calcium MS/MSD High analyte concentrations 190343-002E Magnesium MS/MSD High analyte concentrations 190343-002E Sodium MS/MSD High analyte concentrations 1906343-000lD Ammonia MS/MSD Sample matrix interference Duplicate (DUP): The parameters that required a duplicate analysis had RPDs within the control limits, with the following exception: The RPD for TDS on sample 1906343-00lC was outside of control limits due to suspected sample non- homogeneity or matrix interference. Corrective Action: None required. Report Date: 7/5/2019 Page 4 of35 All an.ti) ses applicable to lhe CWA. SDWA. and RCRA are performed in accordance Lo NELAC protocols Peninenl sampling information is localed on the atlached CDC Confidential Business Information: This report is prm ided for the exclLLSi\ e use of the ~cldressee P1i, ile~es o.r sub,_seq~enl ~1~e ol the ~'.":'1e of this 0 COJ~pan) or ru1) 1~mber of its slaff. or reproductio1~ ~r 1his repo~ in .con~ecl,on~ \\ilh 1he n~, ertisement. p~omolio.n m sale or ?1~) ~· od~cl or p1.ocess, ~r in ~onn~c.Lion \\'(th 1h~ r~·publicalion or this report Volatile Case Narrative American West Client: ANALYTICAL LA80RATORIE8 Energy Fuels Resources, Inc. Tanner Holliday 3440 South 700 West ;alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax : (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Contact: Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-0-C Discrepancies: Method: Analysis: Seeps and Springs 2019 1906343 6/13/2019 6/11/2019 Intact None SW-846 8260C/5030C Volatile Organic Compounds General Set Comments: One target analyte was observed above its reporting limit. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPO, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike/ Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 7/5/2019 Page 5 of 35 All anol~·ses applicable lo the CWA_ SDWA. and RCRA are perfom1ed in accordance to NELAC p1olocols Pertinenl sampling informnt,on is located on the attached COC Conlidentinl Business Jnformalion: This report is provided for the exclusi\e use or the ~ddressee Pri\ ile~es o_f sub..5eq~nl ~1~e of Lhe ~~e of lh1s .con_1pcm~ or M~ n.2_7mbe1 or its slnff, or reµroductio.~ ~rthis repo~ in ~ot~lection,. \\ilh the~' ertiseme11L. p~omotio.n ~r sale or:"!~ ~rod~ct or p1.ocess, ~fin 7°nn~c~ion w!lh 1h~ r~-publiciltion or !his repor1 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West _QC SUMMARY REPORT ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 1906343 Dept: ME Project: Seeps and Springs 2019 QC Type: LCS ---------- Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: LCS-63253 Date Analyzed: 06/28/2019 1505h Test Code: 200.7-DIS Date Prepared: 06/14/2019 1410h Calcium 10.7 mg/L E200.7 0.0937 1.00 10.00 0 107 85 • 115 Magnesium 11.2 mg/L E200.7 0.0439 1.00 10.00 0 112 85 -115 Potassium 10.9 mg/L E200.7 0.134 1.00 10.00 0 109 85 -115 Sodium 11.3 mg/L E200.7 0.187 1.00 10.00 0 113 85 -115 Vanadium 0.220 mg/L E200.7 0.00138 0.00500 0.2000 0 110 85 • 115 Lab Sample ID: LCS-63254 Date Analyzed: 06/17/2019 1339h Test Code: 200.8-DIS Date Prepared: 06/14/20191410h Arsenic 0.211 mg/L E200.8 0.000298 0.00200 0.2000 0 106 85 -115 Beryllium 0.209 mg/L E200.8 0.000198 0.00200 0.2000 0 105 85 -115 Cadmium 0.207 mg/L E200.8 0.0000858 0.000500 0.2000 0 103 85 -115 Chromium 0.213 mg/L E200.8 0.00191 0.00200 0.2000 0 107 85 -115 Cobalt 0.210 mg/L E200.8 0.000300 0.00400 0.2000 0 105 85 -115 Copper 0.214 mg/L E200.8 0.00282 0.00200 0.2000 0 107 85 -115 Iron 1.05 mg/L E200.8 0.0496 0.100 1.000 0 105 85 -115 Lead 0.199 mg/L E200 8 0.000448 0.00200 0.2000 0 99.3 85 -115 Manganese 0.215 mg/L E200.8 0.00108 0.00200 0.2000 0 108 85 -115 Molybdenum 0.213 mg/L E200.8 0.000652 0.00200 0.2000 0 106 85 -115 Nickel 0.211 mg/L E200.8 0.00148 0.00200 0.2000 0 105 85 -115 Selenium 0.220 mg/L E200.8 0.000574 0.00200 0.2000 0 110 85 -115 Silver 0.201 mg/L E200.8 0.000232 0.00200 0.2000 0 100 85 -115 Thallium 0.197 mg/L E200.8 0.000154 0.00200 0.2000 0 98.6 85 -115 Tin 1.05 mg/L E200.8 0.00116 0.00400 1.000 0 105 85 -115 Uranium 0.211 mg/L E200.8 0.000176 0.00200 0.2000 0 105 85 -115 -Lab Sample ID: LCS-63254 Date Analyzed: 06/17/2019 1924h Test Code: 200.8-DIS Date Prepared: 06/14/2019 1410h Zinc 1.02 mg/L E200.8 0.00418 0.00600 1.000 0 102 85 -115 Report Date: 7/5/2019 Page 19 of35 analyses applicable to the CWA. SOWA, and RCRA are performed in accordance to NE LAC protocols Pertinent sampling information is located on the attached COC Confidential Business lnfonnation: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tl- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be blfanted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1906343 Project: Seeps and Springs 20 I 9 Analyte Result Lab Sample ID: LCS-63387 Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury 0.00317 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 06/24/2019 746h 06/21 /2019 1450h mg/L E245.l 0.0000396 0.0000900 0.003330 Tanner Holliday ME LCS Spike Ref. Amount %REC 0 95.2 Limits 85 -115 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 7/5/201 9 Page 20 of35 analyses applicable to the CWA. SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling infom1ation is located on the attached COC. Confidential Business [nfonnation: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process_ or in connection wlth the re-publication of this report for any purpose other than for the addressee will be b>Tanted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1906343 Project: Seeps and Springs 2019 Analyte Result Lab Sample ID: MB-63253 Date Analyzed: Test Code: 200.7-DIS Date Prepared: Calcium < 1.00 Magnesium < 1.00 Potassium < 1.00 Sodium < 1.00 Vanadium < 0.00500 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com QC SUMMARY REPORT Contact: Tanner Holliday Dept: ME QC Type: MBLK Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 06/28/2019 1501h 06/14/2019 1410h mg/L E200.7 0.0937 1.00 mg/L E200.7 0.0439 1.00 mg/L E200.7 0.134 1.00 mg/L E200.7 0.187 1.00 mg/L E200 7 0.00138 0.00500 -Lab Sample ID: MB-63254 Date Analyzed: 06/17/2019 1336h Test Code: 200.8-DIS Date Prepared: 06/14/2019 1410h Arsenic < 0.000200 mg/L E200.8 0.0000298 0.000200 Beryllium < 0.000200 mg/L E200.8 0.0000198 0.000200 Cadmium < 0.0000500 mg/L E200.8 0.00000858 0.0000500 Chromium < 0.000200 mg/L E200.8 0.000191 0.000200 Cobalt < 0.000400 mg/L E200.8 0.0000300 0.000400 Copper < 0.000200 mg/L E200.8 0.000282 0.000200 Iron < 0.0100 mg/L E200.8 0.00496 0.0100 Lead < 0.000200 mg/L E200.8 0.0000448 0.000200 Manganese < 0.000200 mg/L E200.8 0.000108 0.000200 Molybdenum < 0.000200 mg/L E200.8 0.0000652 0.000200 Nickel < 0.000200 mg/L E200 8 0.000148 0.000200 Selenium < 0.000200 mg/L E200.8 0.0000574 0.000200 Silver < 0.000200 mg/L E200.8 0.0000232 0.000200 Thallium < 0.000200 mg/L E200.8 0.0000154 0.000200 Tin < 0.000400 mg/L E200.8 0.000116 0.000400 Uranium < 0.000200 mg/L E200.8 0.0000176 0.000200 Lab Sample ID: MB-63254 Date Analyzed: 06/17/2019 1921h Test Code: 200.8-DIS Date Prepared: 06/14/2019 1410h Zinc < 0.000600 mg/L E200 8 0.000418 0.000600 Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit Qual Report Date: 7/5/2019 Page 21 of35 analyses applicable to the CWA. SOWA, and RCRA are perfom,ed in accordance to NE LAC protocols Pertinent sampling infom1ation is located on the attached COC Confidential Business [nformation: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1906343 Project: Seeps and Springs 2019 Analyte Result Lab Sample ID: MB-63387 Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury < 0.0000900 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 06/24/2019 744h 06/21/2019 1450h mg/L E245.l 0.0000396 0.0000900 Tanner Holliday ME MBLK Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual Report Date: 7/5/2019 Page 22 of35 analyses applicable to the CWA, SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC. Confidential Business rnformation: This report is provided for the exclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 Laboratory Director e-mail: awal@ awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West _QC SUMMARY REPORT ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 1906343 Dept: ME Project: Seeps and Springs 2019 QC Type: MS Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt 0/o RPD Limit Qual Lab Sample ID: 1906343-00ZEMS Date Analyzed: 06/28/2019 1514h Test Code: 200.7-DIS Date Prepared: 06/14/2019 1410h Calcium 161 mg/L E200.7 0.937 10.0 10.00 165 -31.5 70 • 130 Magnesium 43.8 mg/L E200 7 0.439 10.0 10.00 45.6 -17.7 70 • 130 Sodium 127 mg/L E200.7 1.87 10.0 10.00 128 -5.56 70 • 130 Lab Sample ID: 1906343-00ZEMS Date Analyzed: 06/28/2019 1710h Test Code: 200.7-DIS Date Prepared: 06/14/2019 1410h Potassium 14.1 mg/L E200.7 0.134 1.00 10.00 3.31 108 70 • 130 Vanadium 0.217 mg/L E200.7 0.00138 0.00500 0.2000 0 108 70 • 130 Lab Sample ID: 1906343-00ZEMS Date Analyzed: 06/17/20191354h Test Code: 200.8-DIS Date Prepared: 06/14/2019 1410h Arsenic 0.208 mg/L E200.8 0.000298 0.00200 0.2000 0.000569 104 75 • 125 Beryllium 0.203 mg/L E200.8 0.000198 0.00200 0.2000 0 101 75 • 125 Cadmium 0.200 mg/L E200,8 0.0000858 0.000500 0.2000 0 99.9 75 • 125 Chromium 0.206 mg/L E200.8 0.00191 0.00200 0.2000 0 103 75 • 125 Cobalt 0.201 mg/L E200,8 0.000300 0.00400 0.2000 0 101 75 • 125 Copper 0.204 mg/L E200.8 0.00282 0.00200 0.2000 0 102 75 • 125 Iron 1.02 mg/L E200.8 0.0496 0.100 1.000 0 102 75 • 125 Lead 0.193 mg/L E200.8 0.000448 0.00200 0.2000 0 96.3 75 • 125 Manganese 0.209 mg/L E200.8 0.00108 0.00200 0.2000 0 105 75 -125 Molybdenum 0.231 mg/L E200.8 0.000652 0.00200 0.2000 0.0202 105 75 • 125 Nickel 0.202 mg/L E200.8 0.00148 0.00200 0.2000 0 101 75 • 125 Selenium 0.227 mg/L E200.8 0.000574 0.00200 0.2000 0.0108 108 75 • 125 Silver 0.190 mg/L E200 8 0.000232 0.00200 0.2000 0.00114 94.2 75 • 125 Thallium 0.192 mg/L E200.8 0.000154 0.00200 0.2000 0 96.0 75 • 125 Tin 1.05 mg/L E200.8 0.00116 0.00400 1.000 0 105 75 • 125 Uranium 0.216 mg/L E200 8 0.000176 0.00200 0.2000 0.00904 104 75 -125 Report Date: 7/5/2019 Page 23 of 35 analyses applicable to the CWA. SDWA, and RCRA are performed ln accordance to NE LAC protocols Pertinent sampling infom1ation is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with there-publication of this report for any purpose other than for the addressee will be granted only on contact. This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1906343 Project: Seeps and Springs 2019 Analyte Result Lab Sample ID: 1906343-002EMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Zinc 1.02 Lab Sample ID: I906343-002EMS Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury 0.00327 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 06/17/20191933h 06/14/2019 1410h mg/L E200.8 0.00418 0.00600 1.000 06/24/2019 7 54h 06/21/2019 1450h mg/L E245.l 0.0000396 0.0000900 0.003330 Tanner Holliday ME MS Spike Ref. Amount %REC 0.0068 101 0 98.2 2 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD. Limits 75 -125 85 -115 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit Qua! Report Date: 7/5/2019 Page 24 of35 analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NE LAC protocols Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer ANALYTICAL LABORATORIES _QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 1906343 Dept: ME Project: Seeps and Springs 2019 QC Type: MSD ---- Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 1906343-002EMSD Date Analyzed: 06/28/2019 1516h Test Code: 200.7-DIS Date Prepared: 06/14/2019 1410h Calcium 164 mg/L E200.7 0.937 10.0 10.00 165 -8.21 70 -130 161 1.43 20 2 Magnesium 46.4 mg/L E200.7 0.439 10.0 10.00 45.6 8.40 70 -130 43.8 5.79 20 Sodium 128 mg/L E200.7 1.87 10.0 10.00 128 0.626 70 • 130 127 0.485 20 Lab Sample ID: 1906343-002EMSD Date Analyzed: 06/28/2019 1708h Test Code: 200.7-DIS Date Prepared: 06/14/2019 1410h Potassium 14.3 mg/L E200.7 0.134 1.00 10.00 3.31 110 70 • 130 14.1 1.09 20 Vanadium 0.214 mg/L E200,7 0.00138 0.00500 0.2000 0 107 70 • 130 0.217 1.54 20 Lab Sample ID: 1906343-002EMSD Date Analyzed: 06/17/2019 1358h Test Code: 200.8-DIS Date Prepared: 06/14/2019 1410h Arsenic 0.206 mg/L E200.8 0.000298 0.00200 0.2000 0.000569 103 75 • 125 0.208 1.21 20 Beryllium 0.201 mg/L E200.8 0.000198 0.00200 0.2000 0 100 75 -125 0.203 0.927 20 Cadmium 0.196 mg/L E200.8 0.0000858 0.000500 0.2000 0 98.1 75 • I 25 0.2 1.80 20 Chromium 0.208 mg/L E200.8 0.00191 0.00200 0.2000 0 104 75 • 125 0.206 1.17 20 Cobalt 0.201 mg/L E200.8 0.000300 0.00400 0.2000 0 101 75 -125 0.201 0.118 20 Copper 0.203 mg/L E200.8 0.00282 0.00200 0.2000 0 102 75 • 125 0.204 0.150 20 Iron 1.02 mg/L E200.8 0.0496 0.100 1.000 0 102 75 • 125 1.02 0.367 20 Lead 0.190 mg/L E200.8 0.000448 0.00200 0.2000 0 95.1 75 -125 0.193 1.27 20 Manganese 0.209 mg/L E200.8 0.00108 0.00200 0.2000 0 104 75 -125 0.209 0.313 20 Molybdenum 0.228 mg/L E200.8 0.000652 0.00200 0.2000 0.0202 104 75 -125 0.231 1.15 20 Nickel 0.204 mg/L E200,8 0.00148 0.00200 0.2000 0 102 75 • 125 0.202 0.659 20 Selenium 0,224 mg/L E200.8 0.000574 0.00200 0.2000 0.0108 106 75 -125 0.227 1.38 20 Silver 0.189 mg/L E200 8 0.000232 0.00200 0.2000 0.00114 94.1 75 -125 0.19 0.157 20 Thallium 0.191 mg/L E200.8 0.000154 0.00200 0.2000 0 95.4 75 -125 0.192 0.603 20 Tin 1.04 mg/L E200.8 0.00116 0.00400 1.000 0 104 75 • 125 1.05 1.31 20 Uranium 0.215 mg/L E200.8 0.000176 0.00200 0.2000 0.00904 103 75 -125 0.216 0.417 20 Report Date: 7/5/2019 Page 25 of 35 analyses applicable to the CWA. SOWA, and RCRA are perfom,ed in accordance to NELAC protocols Pertinent sampling mfonnation is located on the attached COC Confidential Business Information This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt- ne of this company or any member of its staff, or reproduction of this report In connection with the advertisement promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1906343 Project: Seeps and Springs 2019 Analyte Result Lab Sample ID: l 906343-002 EMSD Date Analyzed: Test Code: 200.8-DIS Date Prepared: Zinc 1.02 Lab Sample ID: 1906343-002EMSD Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury 0.00324 3440 South 700 West Salt Lake City, UT 84 I I 9 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 06/17/2019 1936h 06/14/2019 1410h mg/L E200.8 0.00418 0.00600 1.000 06/24/2019 756h 06/21/2019 1450h mg/L E245.l 0.0000396 0.0000900 0.003330 Tanner Holliday ME MSD Spike Ref. Amount %REC 0.0068 102 0 97.1 2 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD. Limits 75 -125 85 -115 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPO Limit 1.02 0.744 20 0.00327 1.08 20 Qual Report Date: 7/5/2019 Page 26 of35 analyses applicable to the CWA. SOWA, and RCRA are perfom1ed in accordance to NE LAC protocols Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-pub] ication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL Client: Energy Fuels Resources, Inc. Lab Set ID: 1906343 Project: Seeps and Springs 2019 Analyte Result Lab Sample ID: 1906343-00ICDUP Date Analyzed: Test Code: TDS-W-2540C Total Dissolved Solids 1,010 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday WC DUP Spike Ref. Amount %REC 06/14/2019 1100h mg/L SM2540C 16.0 20.0 @ -High RPD due to suspected sample non-homogeneity or matrix interference. Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit 892 12.2 5 Qual @ Report Date: 7/5/2019 Page 27 of35 analyses applicable to the CWA. SOWA, and RCRA are perfom1ed in accordance to NE LAC protocols Pertinent sampling infom1ation is located on the attached COC Confidential Business lnfonnat1on: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tl" ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any producl or process. or in connection with there-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1906343 Project: Seeps and Springs 2019 Analyte Lab Sample ID: LCS-RI27501 Test Code: 300.0-W Chloride Fluoride Sulfate Lab Sample ID: LCS-Rl27013 Test Code: ALK-W-23208-LL Alkalinity (as CaC03) Lab Sample ID: LCS-63399 Test Code: NH3-W-350. l Ammonia (as N) Lab Sample ID: LCS-Rl26960 Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) Lab Sample ID: LCS-Rl27047 Test Code: TDS-W-2540C Total Dissolved Solids Result Date Analyzed: 4.94 4.96 5.31 Date Analyzed: 250 Date Analyzed: Date Prepared: IO.I Date Analyzed: 1.07 Date Analyzed: 182 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 06/27/2019 1959h mg/L E300 0 0.0386 0.100 5.000 mg/L E300.0 0.0240 0.100 5.000 mg/L E300.0 0.174 0.750 5.000 06/17/2019 739h mg/L SM2320B 0.781 1.00 250.0 06/24/2019 l !Olh 06/23/2019 2000h mg/L E350.l 0.0492 0.0500 10.00 06/14/2019 1028h mg/L E353,2 0.00363 0.0100 1.000 06/14/2019 1100h mg/L SM2540C 8.00 10.0 205.0 Tanner Holliday WC LCS Spike Ref. Amount %REC 0 98.8 0 99.1 0 106 0 99.8 0 101 0 107 0 88.8 Limits 90 -110 90 -110 90 -110 90 -110 90 -110 90-110 80 -120 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual Report Date: 7/5/2019 Page 28 of35 analyses applicable to the CWA, SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling infomiation is located on the attached COC. Confidential Business lnformation: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re~publication of this report for any purpose other than for the addressee will be granted only on contact. This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1906343 Project: Seeps and Springs 2019 Analyte Result Lab Sample ID: MB-Rl27501 Date Analyzed: Test Code: 300.0-W Chloride < 0.100 Fluoride < 0.100 Sulfate < 0.750 Lab Sample ID: MB-Rl27013 Date Analyzed: Test Code: ALK-W-23208-LL Bicarbonate (as CaC03) < 1.00 Carbonate (as CaC03) < 1.00 Lab Sample ID: MB-63399 Date Analyzed: Test Code: NH3-W-350. l Date Prepared: Ammonia (as N) < 0.0500 Lab Sample ID: MB-R126960 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) < 0.0100 Lab Sample ID: MB-Rl27047 Date Analyzed: Test Code: TDS-W-2540C Total Dissolved Solids < 10.0 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 06/27/2019 1942h mg/L E300.0 0.0386 0.100 mg/L E300.0 0.0240 0.100 mg/L E300.0 0.174 0.750 06/17/2019 739h mg/L SM2320B 0.781 1.00 mg/L SM2320B 0.781 1.00 06/24/2019 1100h 06/23/2019 2000h mg/L E350 l 0.0492 0.0500 06/14/2019 1027h mg/L E353 2 0.00363 0.0100 06/14/2019 1100h mg/L SM2540C 8.00 10.0 Tanner Holliday WC MBLK Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit Qual Report Date: 7/5/2019 Page 29 of 35 analyses applicable to the CWA. SOWA, and RCRA are perfom1ed in accordance to N ELAC protocols Pertinent sampling infom,ation is located on the attached COC' Confidential Business Information: This repon is provided for the exclusive use of the addressee Privileges of subsequent use of ti- ne of thls company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This Client: Energy Fuels Resources, Inc. Lab Set ID: 1906343 Project: Seeps and Springs 2019 Analyte Result Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Method MDL Reporting Limit Contact: Dept: QC Type: Amount Spiked Tanner Holliday WC MS Spike Ref. Amount %REC Lab Sample ID: 1906343-00IBMS Date Analyzed: 06/27/2019 2033h Test Code: 300.0-W Chloride Fluoride Sulfate Lab Sample ID: 1906343-00IBMS Test Code: ALK-W-2320B-LL Alkalinity (as CaC03) Lab Sample ID: 1906343-00lDMS Test Code: NH3-W-350.l Ammonia (as N) Lab Sample ID: 1906343-00lDMS Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 209 98.6 262 Date Analyzed: 1,480 Date Analyzed: Date Prepared: 12.1 Date Analyzed: 1.02 mg/L E300.0 0.772 mg/L E300.0 0.480 mg/L E300.0 3.48 06/17/2019 739h mg/L SM2320B 0.781 06/24/2019 1120h 06/23/2019 2000h mg/L E350 I 0.0492 06/14/2019 1120h mg/L E353.2 0.00363 1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. 2.00 2.00 15.0 1.00 0.0500 0.0100 100.0 100.0 100.0 1,000 10.00 1.000 104 0.912 160 480 0.168 0.0125 105 97.7 102 99.6 120 101 Limits 90 -110 90 -110 90 -110 80 -120 90 -110 90 -110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 7/5/2019 Page 30 of 35 analyses applicable to the CWA. SOWA, and RCR.A are performed in accordance to NE LAC protocols Pertinent sampling infom,ation is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tl- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This 3440 South 700 West Salt Lake City, UT 841 I 9 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer _QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 1906343 Dept: WC Project: Seeps and Springs 2019 QC Type: MSD ----- Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual Lab Sample ID: l 906343-00 lBMSD Date Analyzed: 06/27/2019 2049h Test Code: 300.0-W Chloride 207 mg/L E300.0 0.772 2.00 100.0 104 103 90 -110 209 0.907 20 Fluoride 97.3 mg/L E300.0 0.480 2.00 100.0 0.912 96.4 90 -110 98.6 1.29 20 Sulfate 269 mg/L E300 0 3.48 15.0 100.0 160 109 90 -110 262 2.79 20 Lab Sample ID: 1906343-00lBMSD Date Analyzed: 06/17/2019 739h Test Code: ALK-W-2320B-LL Alkalinity (as CaC03) 1,480 mg/L SM2320B 0.781 1.00 1,000 480 100 80 -120 1480 0.406 IO Lab Sample ID: l 906343-00 l DMSD Date Analyzed: 06/24/2019 1126h Test Code: NH3-W-350. I Date Prepared: 06/23/2019 2000h Ammonia (as N) 12.7 mg/L E350 l 0.0492 0.0500 10.00 0.168 125 90 -110 12.1 4.67 IO Lab Sample ID: 1906343-00lDMSD Date Analyzed: 06/14/2019 1121h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.06 mg/L E353.2 0.00363 0.0100 1.000 0.0125 104 90-110 1.02 3.28 10 ' -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Report Date: 7/5/2019 Page 31 of 3 5 analyses applicable to the CWA. SOWA, and RCRA are perforn1ed in accordance to NE LAC protocols Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the e:'Cclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1906343 Project: Seeps and Springs 2019 Analyte Result Lab Sample ID: LCS VOC-3 061319A Date Analyzed: Test Code: 8260-W-DENIOO Benzene 20.5 Chloroform 19.3 Methylene chloride 20.1 Naphthalene 18.2 Tetrahydrofuran 15.6 Toluene 20.2 Xylenes, Total 63.0 Surr: l ,2-Dichloroethane-d4 52.0 Surr: 4-Bromofluorobenzene 51.3 Surr: Dibromofluoromethane 48.0 Surr: Toluene-dB 49.1 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA LCS Spike Ref. Amount %REC 06/13/2019 742h µg/L SW8260C 0.147 1.00 20.00 0 103 µg/L SW8260C 0.166 1.00 20.00 0 96.6 µg/L SW8260C 0.448 1.00 20.00 0 IOI µg/L SW8260C 0.704 LOO 20.00 0 91.2 µg/L SW8260C 0.436 LOO 20.00 0 77.9 µg/L SW8260C 0.177 1.00 20.00 0 IOI µg/L SW8260C 0.253 1.00 60.00 0 105 µg/L SW8260C 50.00 104 µg/L SW8260C 50.00 103 µg/L SW8260C 50.00 95.9 µg/L SW8260C 50.00 98.3 Limits 82 -132 85 -124 65 -154 63 -129 59 -125 69 -129 66 -124 80 -136 85 -121 78 -132 81 -123 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 7/5/2019 Page 32 of35 analyses applicable to the CWA. SOWA, and RCRA are perfonned in accordance to NE LAC protocols Pertinent sampling information is located on the attached COC' Confidential Business Information: This report ls provided for the exclusive use of the addressee Privlleges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1906343 Project: Seeps and Springs 2019 Analyte Result Lab Sample ID: MB VOC-3 061319A Date Analyzed: Test Code: 8260-W-DENIOO 2-Butanone <20.0 Acetone <20.0 Benzene < 1.00 Carbon tetrachloride < 1.00 Chloroform < 1.00 Chloromethane < 1.00 Methylene chloride < 1.00 Naphthalene < 1.00 Tetrahydrofuran < 1.00 Toluene < 1.00 Xylenes, Total < 1.00 Surr: l ,2-Dichloroethane-d4 49.0 Surr: 4-Bromofluorobenzene 53.9 Surr: Dibromofluoromethane 44.1 Surr: Toluene-d8 50.5 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA MBLK Spike Ref. Amount %REC 06/13/2019 802h µg/L SW8260C 1.31 20.0 µg/L SW8260C 2.87 20.0 µg/L SW8260C 0.147 1.00 µg/L SW8260C 0.262 1.00 µg/L SW8260C 0.166 1.00 µg/L SW8260C 0.832 1.00 µg/L SW8260C 0.448 1.00 µg/L SW8260C 0.704 1.00 µg/L SW8260C 0.436 1.00 µg/L SW8260C 0.177 1.00 µg/L SW8260C 0.253 1.00 µg/L SW8260C 50.00 98.1 µg/L SW8260C 50.00 108 µg/L SW8260C 50.00 88.2 µg/L SW8260C 50.00 IOI Limits 80 -136 85 -121 78 -132 81 -123 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPO Amt %RPO Limit Qual Report Date: 7/5/2019 Page 33 of35 analyses applicable to the CWA, SOWA, and RCRA are performed in accordance to NE LAC protocols Pertinent sampling infom,ation is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tl- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact_ This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1906343 Project: Seeps and Springs 2019 Analyte Lab Sample ID: 1906343-00IAMS Test Code: 8260-W-DENIOO Benzene Chloroform Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Result Date Analyzed: 19.4 18.2 18.9 17.6 12.1 22.0 56.3 53.5 51.2 48.5 44.1 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA MS Spike Ref. Amount %REC 06/13/2019 1540h µg/L SW8260C 0.147 1.00 20.00 0 97.0 µg/L SW8260C 0.166 1.00 20.00 0 90.9 µg/L SW8260C 0.448 1.00 20.00 0 94.4 µg/L SW8260C 0.704 1.00 20.00 0 88.2 µg/L SW8260C 0436 1.00 20.00 0 60.4 µg/L SW8260C 0.177 1.00 20.00 5.59 82.0 µg/L SW8260C 0.253 1.00 60.00 0 93.9 µg/L SW8260C 50.00 107 µg/L SW8260C 50.00 102 µg/L SW8260C 50.00 97.0 µg/L SW8260C 50.00 88.2 Limits 66 -145 so -146 30 -192 41 -131 43 -146 18 -192 42 -167 72 -151 80 -152 72 -135 80 -124 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit Qual Report Date: 7/5/2019 Page 34 of35 analyses applicable to the CWA. SDWA, and RCRA are perfonned in accordance to NE LAC protocols Pertinent sampling information is located on the attached COC. Confidential Business Information: This repon is provided for the exclusive use of the addressee Privileges of subsequent use of tt- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1906343 Project: Seeps and Springs 2019 Analyte Result Lab Sample ID: 1906343-00 lAMSD Date Analyzed: Test Code: 8260-W-DENlOO Benzene 21.7 Chloroform 19.5 Methylene chloride 18.5 Naphthalene 18.5 Tetrahydrofuran 14.5 Toluene 24.5 Xylenes, Total 58.6 Surr: l ,2-Dichloroethane-d4 55.2 Surr: 4-Bromotluorobenzene 50.8 Surr: Dibromotluoromethane 52.3 Surr: Toluene-d8 48.4 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-labs.com _Q!:_SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA MSD Spike Ref. Amount %REC 06/13/2019 1600h µg/L SW8260C 0.147 1.00 20.00 0 108 µg/L SW8260C 0.166 1.00 20.00 0 97.5 µg/L SW8260C 0.448 1.00 20.00 0 92.3 µg/L SW8260C 0.704 1.00 20.00 0 92.4 µg/L SW8260C 0.436 1.00 20.00 0 72.4 µg/L SW8260C 0.177 1.00 20.00 5.59 94.8 µg/L SW8260C 0.253 1.00 60.00 0 97.7 µg/L SW8260C 50.00 110 µg/L SW8260C 50.00 102 µg/L SW8260C 50.00 105 µg/L SW8260C 50.00 96.8 Limits 66 -145 50 -146 30 -192 41 -131 43 -146 18 -192 42 -167 72 -151 80 -152 72 -135 80 -124 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit 19.4 11.1 25 18.2 7.06 25 18.9 2.30 25 17.6 4.71 25 12.1 18.0 25 22 10.9 25 56.3 4.04 25 Qual Report Date: 7/5/2019 Page 35 of35 analyses applicable to the CWA. SOWA, and RCRA are perfom1ed in accordance to NE LAC protocols Pertinent sampling infom1ation is located on the attached COC Confidential Business fnfom,ation: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This American West Analytical Laboratories Rpt Emailed: UL Denison WORK ORDER Summary Work Order: 1906343 Due Date: 6/27/2019 Page 1 of3 Client: Client ID: Project: Comments: Sample ID 1906343-00IA 1906343-00IB 1906343-00lC 1906343-00ID 1906343-00IE 1906343-002A 1906343-002B 1906343-002C Printed: 06/14/19 17:12 Energy Fuels Resources, Inc. ENE300 Seeps and Springs 2019 Contact: Tanner Holliday QC Level: III WO Type: Project QC 3 (no chromatograms). EDD-Denison. CC KWeinel@energyfuels.com; (USE PROJECT for special DLs). Do not use "*R_" samples as MS/MSD.; Client Sample ID Entrance Seep Ruin Spring Collected Date Received Date Test Code Matrix Sel Storage 6/11/2019 0815h 6/13/2019 1054h 8260-W-DENlOO Aqueous VOCFridge Test Group: 8260-W-DENlOO; #of Analytes: 11 /# of Su": 4 300.0-W df-wc 3 SEL Analytes: CL F S04 ALK-W-2320B-LL df-wc 2 SEL Analytes: ALKB ALKC TDS-W-2540C df-tds 1 SEL Anal)'tes: TDS NH3-W-350.l df -no2/no3 & nh3 I SEL Analytes: NH3N NH3-W-PR df -no2/no3 & nh3 N02/N03-W-353.2 df -no2/no3 & nh3 1 SELAnal)'tes: N03N02N 200.7-DIS df-met 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR df-met 200.8-DIS df-met 17 SELAnalytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR df-met HG-DW-DIS-245.1 df-met 1 SEL Analytes: HG HG-DW-DIS-PR df-met IONBALANCE df-met 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 6/11/2019 0850h 6/13/2019 1054h 8260-W-DENIOO Aqueous VOCFridge Test Group: 8260-W-DENIOO; # of Analytes: JI I# of Surr: 4 300.0-W df-wc 3 SEL AnalJ,_tes: CL F S04 ALK-W-2320B-LL df-wc 2 SEL Analytes: ALKB ALKC TDS-W-2540C df-tds I SEL Analytes: TDS wQ7 3 3 LABORATORY CHECK: %M D RT D CN D TAT D QC D LUO D HOK ___ HOK __ _ HOK___ COC Emailed. ____ _ WORK ORDER Summary Client: Energy Fuels Resources, Inc. Sample ID Client Sample ID 1906343-002D Ruin Spring l906343-002E 1906343-003A Cottonwood Spring 1906343-003B 1906343-003C 1906343-003D 1906343-003E WorkOrder: 1906343 Due Date: 6/27/2019 Page2of3 Collected Date Received Date Test Code Matrix Set Storage 6/11/2019 0850h 6/13/2019 1054h NHJ-W-350.1 Aqueous 6/11/2019 0950h I SEL Analytes: NH3N NH3-W-PR N02/N03-W-353.2 1 SEL Analytes: N03N02N 200.7-DIS 5 SEL Ana/ytes: CA MG K NA V 200.7-DIS-PR 200.8-DIS 17 SEL Ana/ytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR HG-DW-DIS-245.1 I SEL Analytes: HG HG-DW-DIS-PR IONBALANCE 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 6/13/2019 1054h 8260-W-DENlOO Aqueous Test Gruup: 8260-W-DENIOO; # of A_!lalytes: II/# ofSurr: 4 300.0-W 3 SEL Analytes: CL F S04 ALK-W-2320B-LL 2 SEL Analytes: ALKB ALKC TDS-W-2540C 1 SEL Analytes: TDS NH3-W-350.l l SEL Analytes: NH3N NB3-W-PR N02/N03-W-353.2 I SEL Analytes: N03N02N 200.7-DIS 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR 200.8-DIS 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR HG-DW-DIS-245.1 1 SEL Analy_tes: HG df -no2/no3 & nb3 df -no2/no3 & nb3 df -no2/no3 & nb3 df-met df-met df-met df-met df-met df-met df-met VOCFridge df-wc df-wc df-tds df -no2/no3 & nh3 df -no2/no3 & nb3 df -no2/no3 & nh3 df-met df-met elf-met df-met df-met Printed: 06/14/19 17:12 LABORATORY CHECK: %M O RT O CN O TAT O QC O LUO 0 HOK ___ HOK __ _ HOK___ COC Emailed,__ ___ _ 3 WORK ORDER Summary Work Order: 1906343 Page 3 of3 Client: Energy Fuels Resources, Inc. Due Date: 6/27/2019 Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1906343-00JE Cottonwood Spring 6/11/2019 0950h 6/13/2019 1054h HG-DW-DIS-PR Aqueous df-met IONBALANCE df-met 5 SEL Ana[ytes: BALANCE Anions Cations TDS-Balance TDS-Calc 1906343-004A Back Spring 6/11/2019 0850h 6/13/2019 1054h 8260-W-DENlOO Aqueous VOCFridge 3 Test Group: 8260-W-DENIOO; # of Analytes: 11 /#ofSurr: 4 1906343-004B 300.0-W df-wc 3 SEL Analytes: CL F S04 ALK-W-2320B-LL df-wc 2 SEL Analytes: ALKB ALKC 1906343-004C TDS-W-2540C df-tds I SEL Analytes: TDS 1906343-004D NHJ-W-350.1 df -no2/no3 & nh3 1 SEL Analytes: NH3N NHJ-W-PR df -no2/no3 & nh3 N02/N03-W-353.2 df -no2/no3 & nh3 1 SEL Analytes: N03N02N 1906343-004E 200.7-DIS df-met 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR df-met 200.8-DIS df-met 17 SELAnalytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR df-met HG-DW-DIS-245.1 df-met 1 SEL Analytes: HG HG-DW-DIS-PR df-met IONBALANCE df-met 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 1906343-00SA Trip Blank 6/11/2019 0815h 6/13/2019 1054h 8260-W-DENlOO Aqueous VOCFridge 3 Test Group: 8260-W-DENJOO; # of A~)l_tes: 11 I # of Su": 4 Printed: 06/14/19 17:12 LABORATORY CHECK: %M D RT D CN O TAT O QC D LUO D HOK ___ HOK~--HOK___ COC Emailed. ____ _ 2 3 4 5 6 7 I I ) I ! American West Analytical Laboratories 463 W. 3600 S. Salt lake City, UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 ~ Fax# (801) 263-8687 Email awal@awal~abs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: gpalmc:r@e:ae:rgyftlels.com; KWel.nel@etlergyfuels.com; Email: thoDida~DCJ,a,fucls.com Project Name: Seeps and Springs 2019 Project#: PO#: Sampler Name: Tanner Holliday Date Samole ID: Samoled Entrance Seep 6/11/2019 Ruin Spring 6/11/2019 Cottonwood Spring 6/11/2019 Back Spring 6/11/2019 Trip Blank 6/11/2019 RollnQUSl>8d by: . --\ J:j_/ ~ _,,,.,-Date: 1""1oati.re • . hA >fb,_,. 6112/20ll ..____, ~ ,&,' rnme: PrinlName: T-~m~. 1130 Relinqashod by: UBII}: ""'=tl.Jm 11rne: Print Name: Rellnqulsl)<!dby: '1a!e: IS1ona11.<e -il°"lffle: Print Name: Relinq<ilsllCdby. ----- i,-ate; 1-- / 111me: Prtnj Namo: -' .. I Time Samoled 815 850 950 850 815 Received by: Slanature CHAIN OF CUSTODY All analysis will be conducted using NELAP accredited methods and all data will be reported using AWAL's standard analyte lists and reporting llmlts (POL) unless specifically recuested otherwise on this Chain or Custody and/or attached documentation. QC Level: I Tum Around Time: Unless other arrangements have been made, signed repoos wlll be emailed by 5:00 pm on 3 Standard the day l,ey are due. X Include EDD: 0 LOCUS UPLOAD ::el «l C) EXCEL tiii tiii X Reid Fitered For: --:i:: ::el Dissolved Metals ...... i:: Vi :;E :.f '<!" t'l ~ oi ~ z For Compliance With: c::i & ~ D NELAP c:, D RCRA o' t'l c::i ;:::-;5 >-D CWA c:, ci C) ;:::i D SOWA --O') 0 D ELAP/A2LA ...... ~ c:, g .. Q C) cf 0 r:n D NLLAP ~ c:, ~ .!l k O') c:, C) e:i D Non-Compliance f;j .. ls) Q • D Other: ... 0 ~ 0 -0 t CT' I" l"2. c., CT' = :II C) CII c:, ., f c:, .... c:, u IC C C'> c:, 0 ;J; u 'U ,.; ,.; = t'l ... .. 0 ls) Ill CQ "E ::. fl.I iii .e: r:n .; ~ Known Hazards 0 Ii!: ~ a a ...... ri :i Q) ...... 0 IQ .. u C. cq l'l f1J ~ .. < u & 0 E 0 = ~ ~ .. Q g "' Ii!: Ii!: u i5 0 Samole Comments .. en .. 7 w X x-·x X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 3 w X Cate: Special Instructions: -~ Time: \30Co3t!3 AWAL 1..!b Sample Set# Page 1 of 1 1° 00 ""'(a 1-i:i I\, Laboratory Use Only SamplesWere: l,l.f5 ~ ·~-, .. \•' 2 Amb!lihl Ctilled 3 Temperature D • ~·c 4 Received Brn~ (lmprnperfy y N c:i:Preserved N at bench y N 6 Received Within Qjnmes N lroc Tape Was: G"ent on outer Package N NA ~broken on Outer Package N NA 3 PresentonSample G Y N NA 4 UnbrokenonSample ~) Y N NA Discrepancies Between Sample y N Labels and CCC R~ -----Print Name: Sample containers for metals were field filtered. See the Recetvecl by. Date: Signau.,, ~ Analytical Scope of Work for Reporting Limits and voe analyte Prim Nam~...,........... nrne: list. cedby: Date: ~nature rnme: Print Name: .-. ,, . ' Received by:K:.b, A ti~';» ) Slanature 1 .Al\ 1 I 1 _A Dat~h~ ,C( Print Name, [:::}..e> .,.-,u':-.-~ 'BrtA.u..A\ t'1 111me: \O~_d I Analysis Ammonia COD Cyanide Metals N02& N03 O&G Phenols Sulfide TKN TP04 Procedure: Frequency: Preservation Check Sheet s le Set Ext, Preservative -001 -OffL -oo~ ... oolf oH<2H2S04 11\JO IA//.1 (A,//.} 1/1,(/) oH<2H2S04 0 q , V pH>12NaOH oH<2HN03 vUO l/\,W (M,(} vxa q ~ V V pH<2H2S04 ~ ~ vf,O pH<2HCL 0H<2H2S04 pH>9NaOH, Zn Acetate 0H<2H2S04 pH<2H2S04 Pour a small amount of sample in the sample lid Pour sample from lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid doll 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly"list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + ... # • The sample required additional preservative upon receipt. The sample was received unpreserved. The sample was received unpreserved and therefore preserved upon receipt. The sample pH was unadjustable to a pH < 2 due to the sample matrix. Tl,c, c,n...--1.a. -n.U 'IU"'1t'I n,n.-,,-1;,,c,+n1"lo +" n -ll ......,_ Ano +" +ka. ll"'lnm .... lo """"" ...... ;"' ;...,,..,,... ... l'.o..,o .... ,..o Lab Set ID: I qoto~4~ pH Lot#: t5q Vl .. ------ 0 [§'Jij• I Laboratories LLc a member of The GEL Group INC PO Box 30712 Cr1art est on. SC 29417 2040 Savage Road Charteston. SC 29407 P 843.556.8171 F 843 766.1178 July 10, 2019 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: Analytical for Seeps and Springs 2019 Work Order: 481772 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on June 13, 2019. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies of GEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DWI6138 Enclosures Sincerely, Julie Robinson Project Manager 11111m1 HI u~m 11111111111 t 11111 ge l.co rn Energy Fuels Resources (USA), Inc. Analytical for SDG: 481772 July 10, 2019 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 481772 Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on June 13, 2019 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following samples: Case Narrative: Laboratory ID 481772001 481772002 481772003 481772004 Client ID Entrance Seep Ruin Spring Cottonwood Spring Back Spring Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Julie Robinson Project Manager ~~l,1~ I Sheet1 of 1 CHAIN OF CUSTODY Samples Shipped to: Gel Laboratories Contact: Tanner Hollie ay 2040 Sava9e Road Ph: 435 678 115 Charleston, SC 29407 thollidavtmen ernvfue!s.com Chain of Custody/Sampling Analysis Request Project Samplers Name Sampl ers Signature Seeps and SprinQs 2019 Tanner Holliday I ..=·_)11 Ann 11 jj;//~/ / Time Sample ID Date Collected Collected Laboratory Analysis Re ~uested Entrance Seep 6/11/2019 815 Gross Alpha Ruin Spring 6/11/2019 850 Gross Alpha I Cottonwood Spring 6/11/2019 950 Gross Alpha Back Spring 6/11/2019 850 Gross Alpha I I Comments: Relinquished By:( Signature) Date/Time Received By:(Signature) Date/Time ~ TannJtiJ~-6/12/2019 ~ u2/r3j~q; v ......... ,iJ A ,!On"' -, K-"~ 1130 -Relinquished By:( Signaturef Date/Time Recei~ignature) Date/Time ~. -~~~ .,... ___ g I Laboratories i LC SAMPLE RECEIPT & REVIEW FORM Client: .Ol~tu \ SDG/AR/COC/Work Order: l..\~1112 Recch•ed Bv: ZKW Date Received: to\,~h~ I FedEx Express Circ~c,ble: FedEx Ground • Field Services Courier Other Carrier and Tracking Number t ::;? I 9., -:+ '/'-Ii./ hi q lf1-4Zw~ Suspected lh11.ard Information t 0 *If Nel Counls > I OOcpm on samples not marked "radioaclive", contacl lhe Radial ion S, fc1y Group for further investigation. > 2 Hazard Class Shipped: UNI/: A)Shippcd as a DOT Hazardous? ....... If UN2910, Is lhc Radioactive Shipment Survey Compliant? Yes_ No_ eT ~ ·,if.fi .'. •1r$:~ , r: . . -, !!~ ,t).~.~.:ft:iJl B) Did the client designalc lhe samples arc to be V" OC notn11on,oll;1'liilib.,c11vo.shcil(!ir ·OI\\C,l!nl, ~lOJ'S ct111n J.i/' 11 ffcsfgnu11 n, ' rccei ved as radioacli ve? .,JI'. ·., ~".:."' ""' , . i;, ~ i,, ~ . 'l ' - C) Did 1hc RSO classify 1hc smnples as Maximum Ncl Counls Observed• (Observed Counts -Area Background Counls): ~ ~mRJ•lr radioaclive? ....... Classified as: Rad I Rad 2 Rad 3 ~ ··-=-, -;:.~·. ,\\! ~frfcJ .~ ~~: .1· 1'[ '" 'it,,· D) Did the client designate samples are ~f!re'nQlA . or,hlt7,11(jll(!i . ls J! .,nu cµ-~1\uli)l:h :.j mi lJll~llPI! .,f ~z~ ·~ . . •:ii. ~Ii . hazardous? ...,. j_-• ., a ~ ~i:_,, ~ .... ,,_;:;,·~"-1$!'-_i' ' M.:; lfD or Eis yes, select Ha,.ards below. E) Did lhe RSO identify possible hazards? v h'CB's Flammable Foreign Soil RCRA Asbes1os Beryllium 01her: Sample Rccci11t Criteria ~ < 0 Comment,/Qualilicrs (Required for Non-Conformi g Items) ;;.. z z Shipping containers received imact and Circle Applicable: Seals broken Damaged conlaincr Leaking co111aincr Other (dcsc ibe) I scaled? 2 Chain or custody documenls included Circle Applicable: Client contaclcd and provided COC COC created upon receipt with shipment? --Samples requiring cold preservation Preservation Method: Wet Ice Ice Packs Dry ice ~Other: I TEMP: "Z-S ('.'._ 3 •all tempcralures arc recorded in Celsius within (0 < 6 deg. C)?* Daily check performed and passed on JR Temperature Device Serial II; IR3-18 4 temperature gun? Secondary Te111pcra1ure Device Serial II (If Applicable): Circle Applicoble: Seals broken Damaged conrnincr Lcaki11g c.on1niner Oihcr (dcsc ibc) 5 Sample conlainers intact and scaled? Samples requiring chemical preservation Sample ID's and Containers Affeclcd: I 6 at proper pH? tr p,.. ..... ,.: .... .1., •• , L.nr#• Ir Yes, are Encores or Soil Kits presertl for solids? Yes No -NA (lfyes, lqke to VOA Frcc1.cr) Do any samples require Volatile Do liquid VOA vials contain acid preservation? Yes No NA (lfunknmyn, select No) 7 Analysis? ..... -Krc liquid VOA vials free ol'headspace'! Yes_ No_ NA __ Sample ID's and conlnincrs nffe:ctcd: !D's and tesls affecled: I 8 Samples received within holding time? Sample ID's on COC match ID's on !D's and conlaincrs affeclcd: I 9 boules? Date & time on COC match date & lime Circle Applicable: No dates on containers No times on containers COCmissin • info Other (describe) 10 on bottles? N limber of containers received match Circle Applicable: No con1aincr counl on COC Olher (describe) II number indicated on COC? 12 Are sample containers identifiable as I lr,i:;_1 . nrnv;.1~.1? 13 COC form is properly signed in Circle Applicable: Nol relinquished Other (describe) relinquished/received sections? Commenls (Use Conlinuation Fonn if needed): PM (or PMA) review: lnilials ---1"'-'-'l'y\---"(_~-Dale~ /14.,1-I ~! q~--"'' ::L_ ,r I GL-CHL-SR-001 Rev 6 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 481772 Client SDG: 481772 Seeps and Springs 2019 Project Manager: Project Name: Purchase Order: Package Level: EDD Format: Julie Robinson DNMI00106 Analytical for DW16138 LEVEL3 EIM_DNMI GELID Client Sample ID Client Sample Desc. 481772001 Entrance Seep 481772002 Ruin Spring 481772003 Cottonwood Spring 481772004 Back Spring Collect Date & Time 11-JUN-19 08:15 11-JUN-19 08:50 11-JUN-19 09:50 11-JUN-19 08:50 Work Order Due Date: 11-JUL-19 Package Due Date: EDD Due Date: QA Due Date: IPKe~ate: Receive Time # of Date & Time Zone Cont. 13-JUN-19 09:50 -2 1 13-JUN-19 09:50 -2 1 13-JUN-19 09:50 -2 1 13-JUN-19 09:50 -2 1 09-JUL-19 11-JUL-19 11-JUL-19 12-JUL-19 Lab Matrix GROUND WATER GROUND WATER GROUND WATER GROUND WATER Report Date: 10-JUL-19 Work Order:481772 Page 1 of 2 Collector: C Prelogin #: 20190486669 Project Workdef ID: 1329132 SDG Status: Closed Logged by: Fax Days to Prelog Lab Field Due Date Process CofC# Group QC QC 19 19 19 19 Client Sample ID Status Tests/Methods Product Reference Fax Date PM Comments Aux Data Receive Codes -001 Entrance Seep -002 Ruin Spring -003 Cottonwood Spring -004 Back Spring REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid Product: GFCTORAL Workdef ID: 1461303 Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Samples: 001, 002, 003, 004 Parmname Check: All parmnames scheduled properly CAS# Parmname Gross Radium Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha In Product Group? No Action Product Name Description Contingent Tests Group Name: Client RDL or PQL & Unit Samples Reporting Units pCi/L Group Reference: Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Parm Included Included Custom Function in Sample? in QC? List? REG y y No GEL Laboratories LLC -Login Review Report Login Requirements: Requirement Include? Comments Peer Review by: ___________ _ Work Order (SDG#), PO# Checked? ____ _ Report Date: 10-JUL -19 Work Order:481772 Page 2 of 2 C of C signed in receiver location? _____ _ List of current GEL Certifications as of IO July 2019 State Certification Alaska 17-018 Arkansas 88-0651 CLIA 42D0904046 California 2940 Colorado SCOOOl2 Connecticut PH-0169 DoD ELAP/ ISO 17025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-15-00283,P330-15-00253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SDWA 90129 Kentucky Wastewater 90129 Louisiana Drinking Water LA024 Louisiana NELAP 03046 (AI33904) Maine 2019020 Maryland 270 Massachusetts M-SC012 Michigan 9976 Mississippi SC00012 Nebraska NE-OS-26-13 Nevada scooo 122019-3 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SCOOOl2 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania NELAP 68-00485 Puerto Rico SCOOOl2 S. Carolina Radiochem 10120002 South Carolina Chemistry 10120001 Tennessee TN 02934 TexasNELAP Tl04704235-19-15 UtahNELAP SC000122018-27 Vermont VT87156 Virginia NELAP 460202 Washington C780 Radiochemistry Technical Case Narrative Energy Fuels Resources SDG #: 481772 Product: GFPC, Total Alpha Radium, Liquid Analytical Method: EPA 903.0 Analytical Procedure: GL-RAD-A-044 REV# 10 Analytical Batch: 1888588 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 481772001 481772002 481772003 481772004 1204312433 1204312434 1204312435 1204312436 1204312437 Client Sample rdentification Entrance Seep Ruin Spring Cottonwood Spring Back Spring Method Blank (MB) 48 l 772004(Back Spring) Sample Duplicate (DUP) 48 l 772004(Back Spring) Matrix Spike (MS) 481772004(Back Spring) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Preparation Information Aliquot Reduced aliquots were reduced due to limited sample volume. Technical Information Recounts Samples 1204312435 (Back SpringMS), 1204312436 (Back SpringMSD) and 1204312437 (LCS) were recounted due to low recovery. The recounts are reported. Samples 1204312434 (Back SpringDUP) and 481772004 (Back Spring) were recounted due to high MDCs. The recounts are reported. Miscellaneous Information Additional Comments The matrix spike and matrix spike duplicate, 1204312435 (Back SpringMS) and 1204312436 (Back SpringMSD), aliquots were reduced to conserve sample volume. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMI001 Energy Fuels Resources (USA), Inc. Client SDG: 481772 GEL Work Order: 481772 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. Review/Validation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: j~ ~ Date: 08 JUL 2019 Name: Theresa Austin Title: Group Leader GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Contact: Ms. Kathy Weinel Workorder: 481772 Parmname NOM Sam le Qual _ C R.ad Gas Flow 3atch 1888588 QC1204312434 481772004 DUP Gross Radium Alpha u 0.201 u Uncertainty +l-0.158 QC1204312437 LCS Gross Radium Alpha 555 Uncertainty QC1204312433 MB Gross Radium Alpha u Uncertainty QCJ204312435 481772004 MS Gross Radium Alpha 4470 u 0.201 Uncertainty +l-0.158 QC1204312436 481772004 MSD Gross Radium Alpha 4470 u 0.201 Uncertainty +l-0.158 Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product 0.478 +l-0.212 505 +l-5 .IO 0.824 +l-0.357 3690 +l-45.0 3640 +l-40.5 Units pCilL pCi/L pCilL pCilL pCilL RPD% NIA 1.41 A B BD C D F H K L M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Reoort Date: July 8, 2019 REC% Rane Anlst NIA LXB3 91.l (75%-125%) 82.5 (75%-125%) 81.4 (0%-20%) Page 1 of Date Time 07102/19 06:1 07101/19 09:4• 06128/19 11 :4· 07101119 09:4 07101/19 09:4 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 481772 Parmname NOM Sam le Units RPD% REC% Ran e Anlst M Matrix Related Failure NIA RPD or %Recovery limits do not apply. NI ND NJ Q R u UI UJ UL X y I\ h See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of ----Date Time NI A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPO not applicable. /\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +I-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. TabE Quality Assurance and Data Validation Tables Table E-1 Holding Time Evaluation •· .. - I: Cottonwood Entrance Back Spring West Water Required Holding Time (duplicate of Ruin Spring I', Spring Seep Ruin Spring) Seep Carbonate 14 days OK OK OK OK OK Bicarbonate 14 days OK OK OK OK OK Calcium 6 months OK OK OK OK OK Chloride 28 days OK OK OK OK OK Fluoride 28 days OK OK OK OK OK Magnesium 6 months OK OK OK OK OK Nitrogen-Ammonia 28 days OK OK OK OK OK Nitrogen-Nitrate 28 days OK OK OK OK OK Potassium 6 months OK OK OK OK OK Sodium 6 months OK OK OK OK OK Sulfate 28 days OK OK OK OK OK pH (s.u.) NIA OK OK OK OK OK TDS 7 days OK OK OK OK OK 6 months (except mercury which is 28 Metals days) OK OK OK OK OK Radiologies 6 months OK OK OK OK OK voes (including THF) 14 days OK OK OK OK OK * -Corral Spring, and Corral Canyon were all dry and no samples were collected. E-2 Laboratory Receipt Temperature Check W~,, Ji 01tGit:{1 ~,cul!!b ~. t, s~ ID Rece~pt Temp AWAL-1906343 o.3°c GEL-481772 NIA AW AL -1903737 0.3°C GEL-475027 NIA NIA= These shipments contained samples for the analysis of Gross Alpha only. Per Table 1 in the approved QAP, samples submitted for Gross Alpha analyses do not have a sample temperature requirement. E-3: Ana lytical Method Check -Routine Samples Parameter QAP/Permit: Method Method li,Jsed by Lab Ammonia ( as N) A4500-NH3 G or E350.1 E350.l Nitrate+ Nitrite (as N) E 353.1 or E353.2 E353.2 Metals E 200.7 or E200.8 E200.7, E200.8 Mercury E200.7 or E200.8 or E245.l I;:245.1 Gross Alpha E900.0 or E900.1 or E903.0 E903.0 voes SW8260B or SW8260C SW8260C Chloride A4500-Cl B, A4500-Cl E, or E300.0 E300.0 Fluoride A4500-F C or E300.0 E300.0 Sulfate A4500-S04 E or E300.0 E300.0 TDS A2540C A2540C Carbonate as C03, Bicarbonate as HC03 A2320B A2320B Calcium, Magnesium, Potassium, Sodium E200.7 E200.7 E-4 Reporting Limit Evaluation Piu,ameter P~D\it-Specilied RL Ammonia (as N) 25 mg/L Nitrate+ Nitrite (as N) 10 mg/L Metals ug/L Arsenic 50 Beryllium 4 Cadmium 5 Chromium 100 Cobalt 730 Copper 1300. Iron 11000 Lead 15 · Manganese 800 Mercury 2 Molybdenum 40 Nickel 100 Selenium 50 Silver 100 Thallium 2 Tin 17000 Uranium 30 Vanadium 60 Zinc 5000 Gross Alpha 15 VOCsug/L Acetone 700 Benzene 5 Carbon tetrachloride 5 Chloroform 70 Chloromethane 30 MEK 4000 Methylene Chloride 5 Naphthalene 100 Tetrahydrofuran 46 Toluene 1000 Xylenes 10000 Major Ions mg/L Chloride 1 Fluoride 4 Sulfate 1 IDS 10 Carbonate as C03, Bicarbonate as HC03 Not Specified Calcium, Magnesium, Potassium, Sodium Not Specified All analyses were reported to the required RLs unless noted in the text. E-5: Trip Blank Evaluation The trip blanks for the 2019 sampling program were nondetect. Dlank .Sample Date Laboratory 1906343 6/11/2019 AWAL 1903737 3/27/2019 AWAL E-6 Duplicate Sample Relative Percent Difference Back Spring Major Ions (mg/I) Ruin Spring (Duplicate of Ruin RPO% Spring) Carbonate <1.0 <l.0 N/C Bicarbonate 202 202 0.0 Calcium 165 157 5.0 Chloride 23.9 23.7 0.8 Fluoride 0.505 0.46 9.3 Magnesium 45.6 35.7 24.4 Nitrogen-Ammonia <0.05 <0.05 N/C Nitrogen-Nitrate 1.56 1.65 5.6 Potassium 3.31 3.30 0.3 Sodium 128 119 7.3 Sulfate 474 455 4.1 TDS 900 816 9.8 Metals (ug/1) Arsenic <5.0 <5.0 N/C Beryllium <0.5 <0.5 N/C Cadmium <0.5 <0.5 N/C Chromium <25 <25 N/C Cobalt <10 <10 N/C Copper <10 <10 NIC Iron <30 <30 N/C Lead <1.0 <1.0 N/C Manganese <10 <10 N/C Mercury <0.5 <0.5 N/C Molybdenum 20.2 18.7 7.7 Nickel <20 <20 N/C Selenium 10.8 9.61 11.7 Silver <10 <10 N/C Thallium <0.5 <0.5 N/C Tin <100 <100 N/C Uranium 9.02 9.01 0.1 Vanadium <15 <15 N/C Zinc <10 <10 N/C Radiologies (pCi/1) Gross Alpha <1.00 <1.00 N/C -voes (ug/L) ,~ Acetone <20.0 <20.0 N/C Benzene <1.00 <l.00 N/C Carbon tetrachloride <1.00 <1 .00 N/C Chloroform <l.00 <i.00 N/C Chloromethane <1.00 <1.00 N/C MEK <20.0 <20.0 N/C Methylene Chloride <1.00 <1.00 N/C E-6 Duplicate Sample Relative Percent Difference 1, Back :Pring tylajor Ions (mg/I) Ruin (!Ding (Duplicate of Ruin RPO% 11 pring) Naphthalene <1.00 <1.00 N/C Tetrahydrofuran <1.00 <1.00 N/C Toluene <1.00 <1.00 N/C Xylenes <1.00 <1.00 N/C N/C = Not Calculated Per the approved QAP, an RPO greater than 20% is acceptable if the reported re ult · are les than 5 times the RL. The ere. ults are provided for information only. * Duplicate eheck reported fer g(O alpha minu RN and U are net %RPO. Caleulated 'lalue rare eased Gn th:e formula ill the appi;c:>'ved GWDP and QAP. E-7 Radiologies Counting Error I Gro AlRha ~bunting Gro Alpha minu Rn & U Error~ Within Sample ID minus Rn & hl Precision (±) 20% GWQS GWQS Cotton,w0od Sprin,g <1.0 0.257 NIA 15 NIA Entrance Seep 2.63 0.455 y 15 NIA Back Spring. ~duplicate of Ruin Sp.ring) <1.0 0.158 NIA 15 NIA Ruin Spiing <1.0 0.106 NIA 15 NIA Wes~wa:ter Seep <1.0 0.270 NIA 15 NIA NIA -The sample results are non-detect and the QAP required checks are not applicable. E-8: Laboratory Matrix QC Matrix Spike % Recovery Comparison MS MSD REC Lab Report Well Analyte %REC %REC Range RPD 1906343 Ruin Spring Calcium* NC NC 70 -130 NC 1906343 Ruin Spring Magnesium* NC NC 70-130 NC 1906343 Ruin Spring Sodium* NC NC 70 -130 NC 1906343 Entrance Seep Ammonia (as N) 120 125 90-110 12.] 1903737 Westwater Seep Sodium* NC NC 70 -130 NC * Recovery was not calculated as the analyte level in the sample was greater than 4 times the spike amount. NA = QC was not performed on an EFRI sample. Laboratory Duplicate % Recovery Comparison Lao II Sample Duplicar~ I ' Re ult R-esull Lab.Repe11t We11 Analyte (,mglL) (mg/L) RPli> % Rl?DRange n 1906343 Entrance Seep TDS 1010 892 12.2 5 Surrogate % Recovery All surrogate recoveries were within the laboratory established acceptance limits. Method/Laboratory Reagent Blank detections All method blank results were within the laboratory established acceptance limits. RPD LIMIT 20 20 20 IO 20 TabF CSV Transmittal Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Goble, Kathy Weinel Tuesday, January 14, 2020 12:43 PM Phillip Goble 'Dean Henderson'; Paul Goranson; David Frydenlund; Terry Slade; Logan Shumway; Scott Bakken Transmittal of CSV Files White Mesa Mill 2019 Annual Seeps and Springs Monitoring 475027.csv; 481772.csv; 1903737-report-EDD.csv; 1906343-report-EDD.csv Attached to this e-mail are the electronic copies of laboratory results for the annual seeps and springs monitoring conducted at the White Mesa Mill during 2019, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel eF --· Energy Fuels Resources (USA) Inc. Kathy Weiner Quality Assurance Manager t: 303.389.4134 It: 303.389.4125 225 Union Blvd., Suite 600 Lakewood, CO 80228 http://www.energyfuels.com This e-mail is intended for the exclusive use of person(s) mentioned as the recipient(s). This message and any attached files with it are confidential and may contain privileged or proprietary information. If you are not the intended recipient(s) please delete this message and notify the sender. You may not use, distribute print or copy this message if you are not the intended recipient(s). 1