DRC-2019-015601 - 0901a06880b7a34d

Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600
Lakewood, CO, US, 80228 303 974 2140 www.cnergyfue ENERGY FUELS
D RC- 201, - 015 6?c)
Div of "Afasr,, Maragament
November 25 ,2019 and Rad:ation Control
Sent VIA OVERNIGHT DELIVERY
Mr. Ty L. Howard
Director
Division of Waste Management and Radiation Control
Utah Department of Environmental Quality
195 North 1950 West
P.O. Box 144850
Salt Lake City, UT 84116
NOV 2 6 2019
Re: Transmittal of Annual Tailings System Wastewater Monitoring Report
Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill
Dear Mr. Howard:
Enclosed are two copies of the White Mesa Uranium Mill Annual Tailings System Wastewater
Monitoring Report for 2019 as required by the Groundwater Quality Discharge Permit UGW370004,
as well as two CDs each containing a word searchable electronic copy of the report.
If you should have any questions regarding this report please contact me.
Yours very truly,
J4 _4-3LA-e
ENERGY FUELS RESOURCES (USA) INC.
Kathy Weinel
Quality Assurance Manager
cc: Scott A. Bakken
Terry Slade
Dave Frydenlund
Logan Shumway
Paul Goranson
November 25 ,2019
Sent VIA OVERNIGHT DELIVERY
Mr. Ty L. Howard
Director
Division of Waste Management and Radiation Control
Utah Department of Environmental Quality
195 North 1950 West
P.O. Box 144850
Salt Lake City, UT 84116
Energy Fuels Resources (USA) Inc.
225 Union Blvd. Suite 600
Lakewood, CO, US, 80228
303 974 2140
www. n rgyfuel. .com
Re: Transmittal of Annual Tailings System Wastewater Monitoring Report
Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill
Dear Mr. Howard:
Enclosed are two copies of the White Mesa Uranium Mill Annual Tailings System Wastewater
Monitoring Report for 2019 as required by the Groundwater Quality Discharge Permit UGW370004,
as well as two CDs each containing a word searchable electronic copy of the report.
If you should have any questions regarding this report please contact me.
Yours very truly,
ENERGY FUELS RESOURCES (USA) INC.
Kathy Weinel
Quality Assurance Manager
cc: Scott A. Bakken
Terry Slade
Dave Frydenlund
Logan Shumway
Paul Goranson
White Mesa Uranium Mill
2019 Annual Tailings System Wastewater Sampling
Report
State of Utah
Groundwater Discharge Permit No. UGW370004
Prepared by:
Energy Fuels Resources (USA) Inc.
225 Union Boulevard, Suite 600
Lakewood, CO 80228
November 25, 2019
TABLE OF CONTENTS
1.0 INTRODUCTION .................................................................................................................... 1
2.0 SUMMARY OF MILL TAILINGS SYSTEM ACTNITIES IN 2019 .................................... 1
2.1 Cell 1 ..................................................................................................................................... 2
2.2 Cell 2 ..................................................................................................................................... 2
2.3Cell3 ..................................................................................................................................... 2
2.4 Cell 4A .................................................................................................................................. 2
2.5 Cell 4B .................................................................................................................................. 2
3.0 SAMPLING EVENTS AND SAMPLING METHODOLOGY .............................................. 2
3.1 Sampling Events ................................................................................................................... 2
3.2 Field Data .............................................................................................................................. 3
3.3 Sampling Methodology, Equipment and Decontamination Procedures ............................... 3
3.3.1 Cells ............................................................................................................................... 3
3.3.2 Cell 2 Slimes Drain ........................................................................................................ 4
3.3.3 Cell 4A Leak Detection Systems ................................................................................... 4
3.3.4 Cell 4B Leak Detection Systems ................................................................................... 4
3.3.5 Cells 1, 2, 3, ................................................................................................................... 4
3.4 Field QC Samples ................................................................................................................. 4
3.5 Laboratory Results ................................................................................................................ 5
4.0 QUALITY ASSURANCE AND DATA EVALUATION ....................................................... 5
4.1 Adherence to Sampling Plan and Permit Requirements ....................................................... 5
4.2 Analyte Completeness Review ............................................................................................. 6
4.3 Data Validation ..................................................................................................................... 6
4.3.1 Field Data QNQC Evaluation ....................................................................................... 6
4.3.2 Holding Time Evaluation ............................................................................................... 6
4.3.3 Laboratory Receipt Temperature Check ........................................................................ 7
4.3.4 Analytical Method Check .............................................................................................. 8
4.3.5 Reporting Limit Evaluation ........................................................................................... 8
4.3.6 Trip Blank Evaluation .................................................................................................... 9
4.3.7 QNQC Evaluation for Sample Duplicates .................................................................... 9
4.3.8 Radiologic Counting Error ........................................................................................... 10
4.3.9 Laboratory Matrix QC Evaluation ............................................................................... 11
5.0 HISTORIC DATA .................................................................................................................. 12
6.0 SUMMARY AND CONCLUSIONS ..................................................................................... 13
6.1 Cell 1 ................................................................................................................................... 13
6.2 Cell 3 ................................................................................................................................... 13
6.3 Cell 4A ................................................................................................................................ 14
6.4 Cell 4B ................................................................................................................................ 14
6.5 Cell 2 Slimes Drain ............................................................................................................. 15
6.6 Cells 3, 4A and 4B Slimes Drain ........................................................................................ 15
6.7 Cell 2 Leak Detection System ............................................................................................. 15
6.8 Cells 1 and 3 Leak Detection System ................................................................................. 15
6.9 Cell 4A Leak Detection System .......................................................................................... 15
6.10 Cell 4B Leak Detection System ........................................................................................ 16
6.11 Summary and Conclusions of Analytical Results ............................................................. 16
7.0 CORRECTIVE ACTION REPORT ....................................................................................... 17
7 .1 Assessment of Corrective Actions from Previous Period ................................................... 17
8.0 SIGNATURE AND CERTIFICATION ................................................................................. 18
ii
LIST OF TABLES
Table 1 Summary of Tailings System Wastewater Monitoring
INDEX OF TABS
Tab A Tailings and Slimes Drain Field Sheets
Tab B Sample Location Figures
Tab C Laboratory Analytical Reports
Tab D Chemical and Radiological Summary Tables
Tab E Quality Assurance and Data Validation Tables
E-1 Holding Time Evaluation
E-2 Laboratory Receipt Temperature Check
E-3 Analytical Method Check
E-4 Reporting Limit Evaluation
E-5 Trip Blank Evaluation
E-6 QA/QC Evaluation for Sample Duplicates
E-7 Radiologic Counting Error
E-8 Laboratory Matrix QC Evaluation
iii
2019 ANNUAL TAILINGS SYSTEM WASTEWATER SAMPLING REPORT
1.0 INTRODUCTION
This is the 2019 Annual Tailings System Wastewater Sampling Report for the Energy Fuels
Resources (USA) Inc. ("EFRI") White Mesa Mill (the "Mill"), as required under Part I.F.9 of the
Mill's State of Utah Groundwater Discharge Permit No. UGW370004 (the "Permit") and Section
6.0 of the Mill's Sampling and Analysis Plan for The Tailings Management System, Leak
Detection Systems and Slimes Drains, Revision: 3.0, dated July 8, 2016 (the "Sampling Plan")
and approved by the State of Utah Division of Waste Management and Radiation Control
("DWMRC") on August 8, 2016.
Cell solution and slimes drain sampling is required under the Sampling Plan and Part I.E.10 of
the Permit to be conducted on an annual basis in August of each year for the solutions in Cells 1,
3, 4A, and 4B, the solutions in the slimes drains in Cells 2, 3, 4A, and 4B (for Cells 3, 4A and 4B
after the commencement of dewatering), the solutions in the leak detection system ("LDS") in
Cell 4A and 4B and any detected solutions in the LDS in Cells 1, 2, and 3 at the time of the
August Sampling event. The results of the sampling event are required to be reported to the
DWMRC with the Mill's Third Quarter Groundwater Monitoring Report due December 1, of
each year.
2.0 SUMMARY OF MILL TAILINGS SYSTEM ACTIVITIES IN 2019
This section provides a brief description of the Mill's tailings management system, and any
changes that were made as a result of Mill activities during the reporting year. A description of
which systems were sampled is provided in Section 3.0.
The Mill is designed not to discharge to groundwater or surface waters. Instead, the Mill tailings
system utilizes tailings and evaporation cells for disposal, evaporation, and management of Mill
tailings, effluents, and other wastes as indicated below:
• Cell 1: dedicated to evaporation of Mill waste solutions~
• Cell 2: contains Mill tailings and has been closed to tailings disposal since 1995 and
1 le.(2) byproduct materials since 2000. Cell 2 Phase 1 cover placement commenced in
April 2016;
• Cell 3: contains Mill tailings and is in the final stages of filling. It also accepts other
Mill wastes and 1 le.(2) material from in-situ recovery ("JSR") operations;
• Cell 4A: receives Mill tailings and is used for evaporation of Mill solutions; and
• Cell 4B: is used for evaporation of Mill solutions.
1
2.1 Cell 1
Cell 1 is a 55-acre impoundment built in June of 1981. It operates as an evaporation pond which
receives solutions only. Cell 1 is equipped with a LDS. In 2019, Cell 1 received fluid from the
Mill process, storm water run-off, and Mill laboratory waste. The LDS in Cell 1 was dry in 2019.
2.2 Cell 2
Cell 2 is a 67-acre impoundment built in May of 1980. Cell 2 contains Mill tailings and has been
closed to tailings disposal since 1995 and 1 le.(2) byproduct materials since 2000. Cell 2 Phase 1
cover placement commenced in April 2016. Cell 2 is equipped with a LDS and a slimes drain.
The LDS was dry in 2019. As part of closure activities, EFRI began monitoring the slimes drain
system in 2008. The fluid from the slimes drain is pumped to Cell 4A. Cell 2 no longer receives
any solutions or solids.
2.3 Cell 3
Cell 3 is a 71-acre impoundment built in September 1982. Cell 3 is nearly full of solids and is
undergoing pre-closure steps. This cell is equipped with a LDS and a slimes drain. The LDS was
dry in 2019 and the slimes drain system will be monitored once dewatering begins. In 2019, Cell
3 received solid Mill waste and solid 1 le.2 byproduct material from in situ recovery ("ISR")
facilities.
2.4 Cell 4A
Cell 4A is a 40-acre impoundment built in 2008. This cell is equipped with a LDS and a slimes
drain. The slimes drain system will be monitored once dewatering begins. The LDS in Cell 4A
was sampled in 2019, as described below. In 2019, Cell 4A received solutions from the Mill
process, and solid tailings sands.
2.5 Cell 4B
Cell 4B is a 40-acre impoundment built in 2011. It operates as an evaporation pond which
receives solutions only. Cell 4B is equipped with a LDS. In 2019, Cell 4B received fluid from
the Mill process. The LDS in Cell 4B was sampled in 2019, as described below.
3.0 SAMPLING EVENTS AND SAMPLING METHODOLOGY
3.1 Sampling Events
Samples of solutions from Cells 1, 3, 4A, and 4B, the Cell 2 slimes drain and the Cell 4A and
Cell 4B LDSs were collected on August 21, 2019.
2
In accordance with the Permit, OWMRC was notified of the sampling event, and a OWMRC
representative was present for a part of the sampling. The OWMRC representative collected
split sample aliquots.
Maps showing the locations of the solution and slimes drain and, when applicable, LOS
sampling locations are attached under Tab B. Table 1, included in the Tables Tab, provides an
overview of all solution monitoring samples collected during the current period and includes the
sampling date, laboratory report date, and the work order/lab set ID associated with the analytical
data.
The Permit requires that the samples be analyzed for the water quality parameters listed in Table
2 of the Permit and SVOCs.
Additionally, in order to further characterize the radiological constituents and physical properties
of the solution, EFRI conducted voluntary analyses on the August 21, 2019 samples for radium-
226, thorium-228, thorium-230, thorium-232, uranium-233/234, uranium-235/236, uranium-238,
and specific gravity. The additional data from the August 21, 2019 sampling event are included
in separate data tables in Tab 0. The gross alpha results have been evaluated and are included as
required. These additional data are included in this rep01t for informational purposes only. EFRI
may or may not choose to continue these analyses in future sampling events.
3.2 Field Data
Attached under Tab A are copies of all of the field data sheets recorded in association with the
annual tailings system monitoring program. Sampling dates are listed in Table 1.
3.3 Sampling Methodology, Equipment and Decontamination Procedures
As noted in the OWMRC-approved Sampling Plan, Revision 3.0, dated July 8, 2016, field
filtering and preservation of metals and gross alpha sample aliquots was not completed due to
safety concerns associated with the filtering apparatus and the backpressure created by the
increased viscosity of these samples. The gross alpha and metals aliquots were filtered and
preserved as necessary by the analytical laboratory. It is important to note that field preservation
of the samples is to preclude biological growth and prevent the inorganic analytes from
precipitating. Based on past field data, the cell solutions and LOS and slimes drain samples are
at a pH of 3.88 or less at the time of collection without additional preservative. The addition of
acidic preservatives in the field would add minimal if any protection from biological growth or
precipitation. The VOC sample aliquots were preserved in the field.
3.3.1 Cells
Cell solution samples were collected at the cell sampling stations shown on the Figures in Tab B
using approved procedures described in the OWMRC-approved Sampling Plan, Section 3.1.2.
3
Disposable or dedicated sampling equipment was used during this sampling event and, as such,
rinsate samples were not required.
3.3.2 Cell 2 Slimes Drain
Once a tailings cell has started the dewatering procedures, a sample will be collected from the
slimes drain system. At this time Cell 2 is the only slimes drain that requires sampling. The
location of the slimes drain for Cell 2 is shown in Tab B. While Cells 3, 4A and 4B are equipped
with slimes drain sample locations, Cells 3 and 4A are still active and Cell 4B is being used as an
evaporation pond, and the slimes drains will not be pumped (and/or sampled) until dewatering
operations have commenced.
The Cell 2 slimes drain, shown on the Figures in Tab B, was sampled using a disposable bailer as
noted in the DWMRC-approved Sampling Plan, Section 3.1.3.
Due to the use of a disposable bailer, a rinsate sample was not required.
3.3.3 Cell 4A Leak Detection Systems
The Cell 4A LDS sample was collected from the sampling station shown on the Figures in Tab B
using a dedicated stainless steel bucket and ladle as noted in the DWMRC-approved Sampling
Plan, Section 3.2.2.
3.3.4 Cell 4B Leak Detection Systems
The Cell 4B LDS sample was collected from the sampling station shown on the Figures in Tab B
using a dedicated stainless steel bucket and ladle as noted in the DWMRC-approved Sampling
Plan, Section 3.2.2.
3.3.5 Cells 1, 2, 3,
The Cells 1, 2, 3 LDSs were not sampled during the 2019 sampling event because the systems
were dry.
3.4 Field QC Samples
The field Quality Control ("QC") samples generated during this sampling event included one
duplicate and one trip blank per shipment to each laboratory which received samples for VOCs.
The duplicate sample (Cell 65) was submitted blind to the analytical laboratory. As previously
stated, no rinsate blanks were collected during this sampling event as only dedicated or
disposable equipment was used for sample collection.
4
3.5 Laboratory Results
All analytical results were provided by one of the Mill's two contract analytical laboratories,
GEL Laboratories ("GEL") or Energy Laboratories ("EL").
The laboratories utilized during this investigation were certified under the Environmental Lab
Certification Program administered by the UDEQ Bureau of Lab Improvement for the analyses
they completed.
The analytical data as well as the laboratory Quality Assurance ("QA")/QC summaries are
included under Tab C.
4.0 QUALITY ASSURANCE AND DATA EVALUATION
The Permit requires that the annual tailings system wastewater sampling program be conducted
in compliance with the requirements specified in the Mill's approved White Mesa Uranium Mill
Groundwater Monitoring Quality Assurance Plan ("QAP"), the approved Sampling Plan and the
Permit itself. To meet these requirements, the data validation completed for the tailings system
wastewater sampling program and discussed in this Section utilized the requirements outlined in
the QAP, the Permit and the approved Sampling Plan as necessary. The Mill Quality Assurance
Manager ("QAM") performed a QA/QC review to confirm compliance of the monitoring
program with the requirements of the Permit, the QAP, and the Sampling Plan. As required, data
QA includes preparation and analysis of QC samples in the field, review of field procedures, an
analyte completeness review, and quality control review of laboratory data methods and data.
Identification of field QC samples that were collected and analyzed is provided in Section 3.4
and 4.3.1. Discussion of adherence to the Sampling Plan is provided in Section 4.1. Analytical
completeness review results are provided in Section 4.2. The steps and tests applied to check
laboratory data QA/QC are discussed in Section 4.3.
The analytical laboratories have provided summary reports of the analytical QA/QC
measurements necessary to maintain conformance with National Environmental Laboratory
Accreditation Conference ("NELAC") certification and reporting protocol. The analytical
laboratory QA/QC Summary Reports, including copies of the Chain of Custody forms for each
set of Analytical Results, follow the analytical results under Tab C. Results of review of the
laboratory QA/QC information are provided under Tab E and discussed in Section 4.3, below.
4.1 Adherence to Sampling Plan and Permit Requirements
On a review of adherence by Mill personnel to the QA/QC requirements, the QAM observed that
QA/QC requirements established in the Permit, the QAP, and the Sampling Plan were met, as
discussed below.
5
4.2 Analyte Completeness Review
All analyses required by the Permit Table 2 were completed. In addition, all cell solution
samples were analyzed for SVOCs as required by the Permit.
It is important to note that the laboratories reported more VOC analytes and SVOC analytes than
are required. The data are included in the data packages included in Tab C. The extra data are
included as required by the GWDP Part H.F.
4.3 Data Validation
The QAP and the Permit identify the data validation steps and data quality control checks
required for the tailings system wastewater monitoring program. Consistent with these
requirements, the QAM performed the following evaluations: a field data QA/QC evaluation, a
receipt temperature check, a holding time check, an analytical method check, a reporting limit
check, a trip blank check, a QA/QC evaluation of sample duplicates, a gross alpha counting error
evaluation and a review of each laboratory's reported QA/QC information. Each evaluation is
discussed in the following sections. Data check tables indicating the results of each test are
provided under Tab E.
4.3.1 Field Data QA/QC Evaluation
The QAM performs a review of all field recorded data to assess adherence with QAP, Permit,
and Sampling Plan requirements. The assessment involved review of the Field Data sheets.
Review of the Field Data Sheets noted that all requirements for field data collection were met.
4.3.2 Holding Time Evaluation
QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding
time checks are provided under Tab E. All samples except as noted below were analyzed within
the required holding time.
Per the analytical method, SVOC samples have two holding times; a 7 day holding time for
extraction of the sample and a 40-day holding time for analysis of the extract. The SVOCs in all
samples were extracted 1-day beyond the method specified holding time of 7 days. The extracts
were analyzed within the 40-day holding time window. This deviation does not affect the quality
or usability of the data because the 7-day holding time is set to prevent the loss of SVOC
compounds due to biological degradation. Based on the data, the cell solutions and LDS and
slimes drain samples were at a pH of 3.88 or less at the time of collection without additional
preservative. The pH of the samples at the time of collection provides protection from biological
degradation.
The holding time for acetone in Cell 2 slimes drain samples were missed. The analysis of
acetone in the Cell 2 slimes required a dilution. The initial analysis was within the holding time
however, the diluted analysis for acetone was completed beyond the holding time. The initial
6
analysis cannot be reported because the concentration cannot be accurately quantified because
the value is above the upper quantitation limit of the instrument calibration. This deviation does
not affect the quality or usability of the data because the 14-day holding time is set to prevent the
loss of VOC compounds due to biological degradation and volatilization. Based on the data, the
cell solutions and LDS and slimes drain samples were at a pH of 3.88 or less at the time of
collection without additional preservative. The pH of the samples at the time of collection
provides protection from biological growth. Volatilization is not expected to affect the samples
because of the stability of the matrix due to the density (high specific gravity).
The holding time for fluoride in the Cell 2 slimes drain sample was missed. The laboratory
noted that the original analysis was analyzed within holding time however the data are from a
recheck analysis that was completed after the holding time expired. The difficult matrix likely
caused this issue. Fluoride analyses are completed using a ion-specific electrode. After a
number of samples, the electrode likely needed cleaning or repair, which would have resulted in
erroneous data. Upon data review, the laboratory noticed the anomaly and reanalyzed the sample
beyond the holding time. This deviation does not affect the quality or usability of the data
because the holding time is set to prevent the loss of fluoride due to biological degradation and
chemical reaction. Based on the data, the cell solutions and LDS and slimes drain samples were
at a pH of 3.88 or less at the time of collection without additional preservative. The pH of the
samples at the time of collection provides protection from biological growth and chemical
reaction.
It is important to note that pH is analyzed by the laboratory and is not measured in the field
because the acidic nature of the samples requires a more robust meter than what is available for
field use. In most circumstances pH is measured at the time of sample collection and a holding
time is not assessed. If pH is not measured at the time of collection, a 15-minute time limit is
set. EL flagged the pH results with an "H" flag because the pH was measured beyond the 15-
minute limit. This does not affect the usability of the data, as the sample matrices are stable and
pH is collected for informational purposes only and there are no compliance criteria for pH
measurements.
4.3.3 Laboratory Receipt Temperature Check
Chain of Custody sheets were reviewed to confirm compliance with the Permit. Sample receipt
temperature checks are provided under Tab E. All samples were received within the required
temperature limit except as noted below.
EL labs subcontracted the SVOC analyses to Eurofins, Denver. EL shipped the samples to
Eurofins and four of the SVOCs were received above the required temperature. The SVOC
samples for Cell 4 LDS, Cell 4B, Cell 4B LDS and Cell 65 (duplicate of Cell 1) were received at
7 .6°C. This deviation does not affect the quality or usability of the data because the temperature
requirements are set to prevent the loss of SVOCs due to biological degradation. Based on the
data, the cell solutions and LDS and slimes drain samples were at a pH of 3 .88 or less at the time
of collection. The pH of the samples at the time of collection provides protection from
biological degradation and the missed temperature requirements do not adversely affect the data.
7
4.3.4 Analytical Method Check
All analytical methods reported by both laboratories were checked against the required methods
specified in Table 1 of the QAP. It is important to note that neither the QAP nor the Permit
specify a method for laboratory pH or conductivity. The QAM verified that the laboratory pH
and conductivity methods used by the laboratory were appropriate and provided accurate data.
Table 1 of the QAP does not specify a method for SVOCs because SVOCs are not routinely
collected in the Mill groundwater samples. The GWDP requires that tailings and slimes drain
samples shall include the SVOCs identified in EPA Method 8270D. The GWDP does not
specify that EPA Method 8270D be used for analysis, only that the compounds specified in that
method be included in the analytical list. All of the SVOCs in the GWDP-specified list were
included in the analytical data however EPA Method 8270C, rather than 8270D, was used to
complete the analyses. It is important to note that an additional SVOC was included in the
analyte list. The extra analyte is included in the data in Tab C.
Analytical method check results are provided in Tab E.
4.3.5 Reporting Limit Evaluation
All analytical method reporting limits reported by both laboratories were checked against the
reporting limits specified in the Permit. Section I.E.4 of the Permit requires the following
Reporting Limits:
"all water quality analyses reported shall have a minimum detection limit or reporting limit
that is less than or equal to the respective:
i. Ground Water Quality Standards ("GWQS") concentrations defined in Table 2 of
this Permit,
ii. For TDS, Sulfate, and Chloride, the Minimum Detection Limit for those
constituents for Cell solution monitoring will be as follows: 1,000 mg/L, 1,000 mg/L,
and 1 mg/L, respectively, and
iii. Lower limits of quantitation for groundwater for semi-volatile organic compounds
listed in Table 2 of EPA Method 8270D, Revision 4, dated February, 2007."
Reporting limits are provided in Tab E. There are several constituents that do not have specified
reporting limits in either the Permit or EPA Method 8270D. The reporting limits established by
the laboratory are reported in the data packages. The reporting limits are comparable to other
analytes in the same method based on the same matrix. The reporting limits used by the
laboratory are considered acceptable based on the matrix and known difficulties caused by the
sample matrix.
8
There are several SVOC compounds that had reporting limits that exceeded the reporting limits
listed in Method 8270D in all samples. Those compounds are:
• 3,3'Dichlorobenzidine -2019 reporting limit= 50 ug/L
• Hexachlorobutadiene -2019 reporting limit = 26 to 30 ug/L
• Hexachloroethane -2019 reporting limit = 26 to 30 ug/L
The laboratory method detection limit ("MDL") for each of these compounds is below the
reporting limits listed above and the MDL is below the specified reporting limit in Method
8270D. If the compounds were detected below the reporting limit but above the MDL, the
laboratory would have rep01ted the data and qualified the result with a "J" as they did for other
compounds (for example MEK in Cell 1). Because the MDLs are below the Method 8270D
specified reporting limits, and because any detections would have been reported, the 2019 data
are comparable to historic data and are usable for the intended purpose.
Two additional reporting limit exceedances were noted. The reporting limits for thallium in Cell
1 and lead in Cell 3 exceeded the GWQSs. These exceedances were likely the result of dilutions
necessary to address the matrix interferences inherent in these samples. The exceedances do not
affect the quality or usability of the data because the results of this sampling provide an
"inventory" of cell composition and are not used for comparison to regulatory limits.
In addition, several sets of sample results had the reporting limit raised for at least one analyte
due to sample dilution. In all cases the reported value for the analyte was higher than the
increased detection limit.
4.3.6 Trip Blank Evaluation
All trip blank results were reviewed to identify any blank contamination. Trip blank evaluations
are provided in Tab E. All trip blank results associated with the samples were less than the
reporting limit for all voes.
4.3.7 QA/QC Evaluation for Sample Duplicates
Section 9.1.4 a) of the QAP states that the relative percent difference (the "RPD") will be
calculated for the comparison of duplicate and original field samples. The QAP acceptance limits
for RPDs between the duplicate and original field sample is less than or equal to 20% unless the
measured results are less than 5 times the required detection limit. This standard is based on the
EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review,
February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for all duplicate
pairs for all analytes regardless of whether or not the reported concentrations are greater than 5
times the required detection limits; however, data will be considered noncompliant only when
the results are greater than 5 times the required detection limit and the RPD is greater than 20%.
RPDs are also only calculated when both the sample and the duplicate report a detection for any
9
given analyte. If only one of the pair reports a detection the RPD cannot be calculated. The
additional duplicate information is provided for information purposes.
All duplicate results were within 20% RPD except for magnesium, potassium, sodium, and gross
alpha in the duplicate pair Cell 1/Cell 65. The gross alpha duplicate results are discussed in
Section 4.3.8 below. The chromium and selenium RPDs were greater than 20%, however the
sample and duplicate results reported for Cell 1/Cell 65 were not five times greater than the RLs,
and, as such, the deviation from the 20% RPD requirement is acceptable.
The magnesium, potassium, and sodium results for the duplicate sample Cell 1/Cell 65 did not
meet the duplicate comparability check. Per the approved QAP, and in response to requests from
DWMRC, a separate corrective action for duplicate RPDs outside of acceptance limits has been
developed. The revised procedure for duplicate results outside of acceptance limits was
implemented. The corrective actions that were taken in accordance with the revised procedure
are as follows: the QAM contacted the Analytical Laboratory and requested a review of the raw
data to assure that there were no transcription errors and the data were accurately reported. The
laboratory noted that the data were accurate and reported correctly. Reanalysis was not
completed as the RPDs above the limit are likely due to interferences caused by the matrix, as
discussed below. There is no effect on the usability of the data due to the duplicate results
exceeding the comparability criteria because the matrix of the sample solution caused the
noncompliance.
Results of the RPD test are provided under Tab E. The radiologic duplicates are discussed in
Section 4.3.8 below.
4.3.8 Radiologic Counting Error
Section 9.14 of the QAP requires that all gross alpha analysis reported with an activity equal to
or greater than the Groundwater Compliance Limit (the "GWCL") (for the tailings system
wastewater samples the GWQS will be used), shall have a counting variance that is equal to or
less than 20% of the reported activity concentration. An error term may be greater than 20% of
the reported activity concentration when the sum of the activity concentration and error term is
less than or equal to the GWQS.
Results of routine radiologic sample QC are provided under Tab E. All tailings system
wastewater radiologic sample results met the counting error requirement.
Section 9.1.4 of the QAP also requires a comparability check between the sample and field
duplicate sample results utilizing the formula provided below:
The original and duplicate sample did not meet the duplicate comparability check specified in the
QAP for gross alpha. Results of the RPD test are provided under Tab E. Per the approved QAP,
and in response to requests from DWMRC, a separate corrective action for duplicate RPDs
10
outside of acceptance limits has been developed and is documented in the revised QAP. The
revised procedure for duplicate results outside of acceptance limits was implemented for the
gross alpha results in duplicate pair Cell 1/Cell 65. The corrective actions that were taken in
accordance with the revised procedure are as follows: the QA Manager contacted the Analytical
Laboratory and requested a review of the raw data to assure that there were no transcription
errors and the data were accurate I y reported. The laboratory noted that the data were accurate
and reported correctly. Reanalysis was not completed as the RPDs above the limit are likely due
to interferences caused by the matrix as discussed below.
The lack of comparability of the gross alpha results is indicative of a matrix inte1ference and
does not affect the usability of the data. Matrix interference is most likely caused by high
concentrations of TDS and other constituents in the sample.
4.3.9 Laboratory Matrix QC Evaluation
Section 9.2 of the QAP requires that the laboratory's QA/QC Manager check the following items
in developing data reports: (1) sample preparation information is correct and complete, (2)
analysis information is correct and complete, (3) appropriate analytical laboratory procedures are
followed, (4) analytical results are correct and complete, (5) QC samples are within established
control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical
requirements have been met, and (8) documentation is complete. In addition to other laboratory
checks described above, EFRI's QAM rechecks QC samples and blanks (items (5) and (6)) to
confirm that the percent recovery for spikes and the relative percent difference for spike
duplicates are within the method-specific required limits, or that the case narrative sufficiently
explains any deviation from these limits. Results of this quantitative check are provided under
Tab E. All lab QA/QC results from both EL and GEL met these requirements. There were QC
results which did not meet laboratory established acceptance limits, as identified in Tab E and
described below.
A significant number of the tailings system wastewater samples had the RL raised for multiple
analytes due to matrix interference and/or sample dilution. RL evaluations are discussed in
Section 4.3.5.
The check samples included at least the following: a method blank, a laboratory control spike
("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the equivalent, where
applicable.
All qualifiers, and the corresponding explanations reported in the QA/QC Summary Reports for
any of the check samples for any of the analytical methods were reviewed by the QAM.
The QAP Section 8.1.2 requires that a MS/MSD pair be analyzed with each analytical batch,
depending upon the analytical method requirements and/or method limitations. The QAP does
not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the
MS/MSD pair be prepared on EFRI samples only. Acceptance limits for MS/MSDs are set by
the laboratories. The review of the information provided by the laboratories in the data packages
11
verified that the QAP requirement to analyze a MS/MSD pair with each analytical batch was
met. While the QAP does not require it, the recoveries were reviewed for compliance with the
laboratory established acceptance limits. The QAP does not require this level of review, and the
results of this review are provided for information only.
The information from the Laboratory QA/QC Summary Reports indicates that the MS/MSDs
recoveries and the associated RPDs were within acceptable laboratory limits for all regulated
compounds.
The QAP specifies that surrogate compounds shall be employed for all organic analyses but the
QAP does not specify acceptance limits for surrogate recoveries. The analytical data associated
with the routine quarterly sampling met the requirement specified in the QAP. The information
from the Laboratory QA/QC Summary Reports indicates that the surrogate recoveries for all
tailings system wastewater samples were within acceptable laboratory limits for all surrogate
compounds except as indicated in Tab E.
There are ten surrogate recoveries outside of acceptance limits for the SVOC analyses. In all
instances the surrogate recoveries outside of acceptance limits were the result of a matrix
interference. A matrix interference resulted in the surrogate compounds being outside of the
acceptance limits noted in Tab E. There are other surrogate compounds used for SVOC analyses
which were all within acceptance limits. As such there is no effect on the quality or usability of
the data. Since surrogate compounds were added to all of the organic analyses as required by the
QAP, the data are compliant with the QAP requirements.
The information from the Laboratory QA/QC Summary Reports indicates that the LCS/LCSD
recoveries for the samples were within acceptable laboratory limits for all LCS/LCSD
compounds except as noted in Tab E. The compounds noted with LCS/LCSD recoveries outside
of acceptance limits are noted for low recovery and the surrogate recoveries associated with the
LCS/LCSD indicate that the analytical system was operating within acceptable limits and the
data are acceptable as reported and there is no effect on the usability of the data.
The QAP, Section 8.1.2 requires that each analytical batch shall be accompanied by a method
blank. The analytical batches routinely contain a blank, which is a blank sample made and
carried through all analytical steps. For the Mill samples, a method blank was prepared for the
analytical methods. Per the approved QAP, contamination detected in analysis of method blanks
will be used to evaluate any analytical laboratory contamination of environmental samples. The
QAP states that non-conformance conditions will exist when contaminant levels in the
samples(s) are not an order of magnitude greater than the blank result. There were no detections
in the method blanks in this quarter. Method blank results are included in Tab E.
5.0 HISTORIC DATA
The historic analytical data for the tailings system wastewater sampling program are included in
Tab D. In addition, the minimum and maximum concentrations compiled in the DWMRC
12
GWDP, Statement of Basis for a Uranium Mining Facility at White Mesa, South of Blanding,
Utah, dated December 1, 2004 are included in Tab D.
6.0 SUMMARY AND CONCLUSIONS
6.1 Cell 1
Cell 1 solutions were acidic in nature with a laboratory pH of 1.14. As expected, the solutions
contained gross alpha, major ions, metals, and Volatile Organic Compounds ("VOCs"). SVOCs
were not detected. Regarding major ions, chloride, fluoride, magnesium, ammonia, potassium,
sodium and sulfate were one or more orders of magnitude greater in concentration than the other
major ions. Metals exhibiting the greatest concentration by at least one order of magnitude
higher than the other metals analyzed included arsenic, cadmium, chromium, cobalt, copper,
iron, lead, manganese, molybdenum, nickel, selenium, uranium, vanadium and zinc. A decrease
was noted in the gross alpha concentration in the August 2019 sample, but it is the same order of
magnitude as the 2018 sample. The variable gross alpha results are being caused by matrix
interference due to the nature of the tailings solution and are not representative of gross alpha
from radium concentrations in the solution. This is evidenced by the results of the voluntary
additional analyses. The results of the voluntary analyses are shown in Tab D.
The concentrations reported in the 2019 sample remained within historic ranges. It is important
to note that not all constituents present in the tailings fluids will exhibit the same behavior as a
result of concentration of the tailings fluids and any increases or decreases in constituent results
will not be linear. The individual constituent results are greatly affected by the matrix of the
tailings fluids and each constituent will behave differently based on the matrix interactions and
the differing solubility properties of the constituent.
Comparison of Cell 1 fluids to those of Cells 4A, and 4B reveals that Cell 1 1s similar in
composition and concentration ratios to the fluids in Cells 4A and 4B.
6.2 Cell 3
Cell 3 solutions were acidic in nature, with a laboratory pH of 3.88. As expected, the solutions
contained gross alpha, major ions, metals, and VOCs. SVOCs were not detected. Regarding
major ions, chloride, fluoride, magnesium, ammonia, sodium and sulfate were generally one or
more orders of magnitude greater in concentration than the other major ions. Metals exhibiting
the greatest concentration by at least one order of magnitude greater than the other metals
analyzed included cadmium, cobalt, copper, iron, manganese, nickel, selenium, uranium,
vanadium and zinc. A decrease in the gross alpha and many metals and ions concentrations was
noted in the August 2019 sample. The reason for the increase in many constituent concentrations
was due to the increased precipitation in early 2019, which would have flowed into Cell 3. As a
result of the additional precipitation, the liquid was diluted. Gross alpha results are not
representative of gross alpha from radium concentrations in the solution. This is evidenced by
the results of the voluntary additional analyses which are shown in Tab D.
13
The concentrations reported in the 2019 sample are similar to previous results. It is important to
note that not all constituents present in the tailings fluids will exhibit the same behavior as a
result of concentration of the tailings fluids and the increases in constituent results will not be
linear. The individual constituent results are greatly affected by the matrix of the tailings fluids
and each constituent will behave differently based on the matrix interactions and the differing
solubility properties of the constituent.
6.3 Cell 4A
Cell 4A solutions were acidic in nature, with a laboratory pH of 2.40. As expected, the solutions
contained gross alpha, major ions, metals, and VOCs. One SVOC was detected. Cell 4A fluid
exhibited the highest major ion concentrations for chloride, fluoride, magnesium, ammonia,
potassium, sodium and sulfate. The metals arsenic, cadmium, chromium, cobalt, copper, iron,
lead, manganese, molybdenum, nickel, selenium, uranium, vanadium and zinc were one or more
orders of magnitude greater than the other metals analyzed. A decrease in the gross alpha
concentration was noted in the 2019 sample. The variable and decreased gross alpha results are
being caused by matrix interference due to the nature of the tailings solution and are not
representative of gross alpha from radium concentrations in the solution. This is evidenced by
the results of the voluntary additional analyses which are shown in Tab D.
Overall, the concentrations reported in the 2019 sample remained approximately the same as the
2018 sample. Concentration changes noted are within the analytical accuracy of the methods
used for analysis. It is important to note that not all constituents present in the tailings fluids
will exhibit the same behavior as a result of concentration of the tailings fluids and the increases
in constituent results will not be linear. The individual constituent results are greatly affected by
the matrix of the tailings fluids and each constituent will behave differently based on the matrix
interactions and the differing solubility properties of the constituent.
Comparison of Cell 4A fluids to those of Cells 1, and 4B reveals that Cell 4A is similar in
composition and concentration ratios to the fluids in Cells 1, and 4B.
6.4 Cell 4B
Cell 4B solutions were acidic in nature, with a laboratory pH of 1.53. As expected, the solutions
contained gross alpha, major ions, metals and VOCs. One SVOCs was detected. Cell 4B fluid
exhibited the highest major ion concentrations for chloride, fluoride, magnesium, potassium,
sodium and sulfate. The metals arsenic, cadmium, chromium, cobalt, copper, iron, lead,
manganese, molybdenum, nickel, selenium, uranium, vanadium and zinc were one or more
orders of magnitude greater than the other metals analyzed. A decrease in the gross alpha
concentration was noted in the 2019 sample, but it is the same order of magnitude as the 2018
sample. The variable gross alpha results are being caused by matrix interference due to the nature
of the tailings solution and are not representative of gross alpha from radium concentrations in
the solution. This is evidenced by the results of the voluntary additional analyses which are
shown in Tab D.
14
The concentrations reported in the 2019 sample remained approximately the same as the 2018
sample. Concentration changes noted are within the analytical accuracy of the methods used for
analysis. It is important to note that not all constituents present in the tailings fluids will exhibit
the same behavior as a result of concentration of the tailings fluids and the increases in
constituent results will not be linear. The individual constituent results are greatly affected by
the matrix of the tailings fluids and each constituent will behave differently based on the matrix
interactions and the differing solubility properties of the constituent.
Comparison of Cell 4B fluids to those of Cells 1, and 4A reveals that Cell 4B is similar in
composition and concentration ratios to the fluids in Cells 1, and 4A.
6.5 Cell 2 Slimes Drain
Cell 2 Slimes drain fluid was acidic in nature, with a laboratory pH of 3.07. As expected, the
solutions contained gross alpha, major ions, metals, and VOCs. Five SVOCs were detected.
Major ions that were highest in concentration by one or more orders of magnitude included
chloride, magnesium, ammonia, sodium and sulfate. For metals, arsenic, cadmium, chromium,
cobalt, copper, iron, manganese, molybdenum, nickel, selenium, uranium, vanadium and zinc
were at least one order of magnitude greater in concentration than other metals analyzed. A slight
decrease in the gross alpha concentration was noted in the 2019 sample. The gross alpha result
decreased but is the same order of magnitude of the historic data. Overall, the concentrations
reported in the 2019 sample remained approximately the same as the 2018 sample.
Concentration changes noted are within the analytical accuracy of the methods used for analysis.
6.6 Cells 3, 4A and 4B Slimes Drain
In accordance with the Permit, the slimes drains for Cell 3, 4A and 4B are not required to be
sampled until dewatering operations have begun. Cell 1 was designed to be used solely as an
evaporation pond and does not have a slimes drain.
6. 7 Cell 2 Leak Detection System
Consistent with the Permit, the Cell 2 LDS was not sampled during the 2019 sampling event.
The Cell 2 LDS is now dry and covered to prevent precipitation inflow.
6.8 Cells 1 and 3 Leak Detection System
Consistent with the Permit, the Cells 1 and 3 leak detection systems were not sampled during the
2019 sampling event because the systems were dry.
6.9 Cell 4A Leak Detection System
Cell 4A LDS solutions were acidic in nature, with a laboratory pH of 2.39. As expected, the
solutions contained gross alpha, major ions, metals and VOCs. One SVOC was detected. Cell
4A LDS fluid exhibited the highest major ion concentrations for chloride, fluoride, magnesium,
15
ammonia, potassium, sodium, and sulfate. The metals arsenic, cadmium, chromium, cobalt,
copper, iron, manganese, molybdenum, nickel, selenium, uranium, vanadium, and zinc were one
or more orders of magnitude greater than the other metals analyzed. An increase in the gross
alpha concentration was noted in the 2019 sample. The variable gross alpha results are being
caused by matrix interference due to the nature of the tailings solution and are not representative
of gross alpha from radium concentrations in the solution. This is evidenced by the results of the
voluntary additional analyses which are shown in Tab D.
Overall, the concentrations reported in the 2019 Cell 4A LDS sample remained within historic
ranges.
6.10 Cell 4B Leak Detection System
Cell 4B LDS solutions were acidic in nature, with a laboratory pH of 1.53. As expected, the
solutions contained gross alpha, major ions, metals, VOCs and one SVOC. Cell 4B LDS fluid
exhibited the highest major ion concentrations for chloride, fluoride, magnesium, ammonia,
potassium, sodium, and sulfate. The metals arsenic, cadmium, chromium, cobalt, copper, iron,
lead, manganese, molybdenum, nickel, selenium, uranium, vanadium and zinc were one or more
orders of magnitude greater than the other metals analyzed. A slight decrease in the gross alpha
concentration was noted in the 2019 sample, but it is the same order of magnitude as the 2018
sample. The variable gross alpha results are being caused by matrix interference due to the nature
of the tailings solution and are not representative of gross alpha from radium concentrations in
the solution. This is evidenced by the results of the voluntary additional analyses which are
shown in Tab D.
Overall, the concentrations reported in the 2019 Cell 4B LDS sample are within historic ranges.
6.11 Summary and Conclusions of Analytical Results
The metals arsenic, cadmium, chromium, cobalt, copper, iron, manganese, molybdenum, nickel,
selenium, uranium, vanadium and zinc were generally present in greatest concentration for all
samples. For major ions, chloride, fluoride, magnesium, ammonia, sodium, and sulfate were
predominant. Both increases and decreases were noted for several metals and major anions.
Concentrations are variable and are driven by Mill operations. EFRI conducted additional
voluntary analyses (not required by the GWDP) in order to further characterize the radiological
and physical properties of the tailings solution, as discussed Section 3 .1 above. The results of the
additional voluntary analyses for radium-226, thorium-228, thorium-230, thorium-232, uranium-
233/234, uranium-235/236, uranium-238, and specific gravity show that the variability in gross
alpha results are being caused by matrix interference due to the nature of the tailings solution and
are not representative of gross alpha from radium concentrations in the solution. EFRI may or
may not choose to continue these additional analyses in the future. The changes in
concentrations of metals and major ions are reflective of Mill operations and are driven by the
addition/movement of fluids during periods of operation. The individual constituent results are
greatly affected by the matrix of the tailings fluids and each constituent will behave differently
based on the matrix interactions and the differing solubility properties of the constituent. Overall,
16
the results of the 2019 tailings solutions are within historic, expected ranges.
7.0 CORRECTIVE ACTION REPORT
No corrective action reports are required for the 2019 annual sampling event.
7.1 Assessment of Corrective Actions from Previous Period
No corrective action reports were required for the 2018 annual sampling event and as such there
is no assessment of previous actions necessary.
17
8.0 SIGNATURE AND CERTIFICATION
This document was prepared by Energy Fuels Resources (USA) Inc.
Energy Fuels Resources (USA) Inc.
By:
Scott A. Bakken Dat '
Senior Director Regulatory Affairs
18
Certification:
I certify, under penalty of law, that this document and all attachments were prepared
under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gather and evaluate the information submitted. Based on my inquiry of the
person or persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fine and imprisonment for knowing violations.
Scott A. Bakken
Senior Director Regulatory Affairs
Energy Fuels Resources (USA) Inc.
19
TABLES
Table 1
Summary of 2019 Tailings System Wastewater Monitoring
Location Sample Date -
Cell 1 Solutions 8/21/2019*
Cell 2 Slimes Drain 8/21/2019*
Cell 3 Solutions 8/21/2019*
Cell 4A Solutions 8/21/2019*
Cell 4A LDS 8/21/2019*
Cell 4B Solutions 8/21/2019*
Cell 4B LDS 8/21/2019*
Cell 65 -Duplicate of 8/21/2019* Cell 1
Notes:
GEL= GEL Laboratories, LLC
EL = Energy Labs
Date of Laboratory Report Work Order Number/Lab Set ID
GEL-09/16/2019 GEL-488668
EL -11/25/2019 EL-C19081073
GEL-09/16/2019 GEL-488668
EL -11/25/2019 EL -C19081073
GEL-09/16/2019 GEL-488668
EL -11/25/2019 EL-C19081073
GEL-09/16/2019 GEL-488668
EL -11/25/2019 EL -C19081073
GEL-09/16/2019 GEL-488668
EL-11/25/2019 EL-C19081073
GEL-09/16/2019 GEL-488668
EL -11/25/2019 EL-C19081073
GEL-09/16/2019 GEL-488668
EL -11/25/2019 EL -C19081073
GEL-09/16/2019 GEL-488668
EL -11/25/2019 EL-C19081073
*EFRI conducted the annual sampling event in August 2019. EFRI collected additional samples aliquots for specific
gravity and additional radiological constituents.
INDEX OF TABS
Tab A Tailings System Monitoring Field Sheets
Tab B Sample Location Figures
Tab C Laboratory Analytical Reports
Tab D Chemical and Radiological Summary Tables
Tab E Quality Assurance and Data Validation Tables
E-1 Holding Time Evaluation
E-2 Laboratory Receipt Temperature Check
E-3 Analytical Method Check
E-4 Reporting Limit Evaluation
E-5 Trip Blank Evaluation
E-6 QNQC Evaluation for Sample Duplicates
E-7 Radiologic Counting Error
E-8 Laboratory Matrix QC Evaluation
Tab A
Tailings System Monitoring Field Sheets
Field Data Record· Tailings Solutions, LDS and Slimes Drain Sampling
Location: ...:C.~e.,:::_,!_\ \_..__ ____ Sampling Personnel: ~1)11ec »0 11:J11.~,o~~n ~m~"'
Oeo.t\ »e.,aef':!)On Mo.rfi Srow(I IOt"I Lc)l'Jlq Is this a Slimes Drain? o Yes ~ No ' 1
If this is a Slimes Drain, measure depth to wastewat~r immediately before sampling.
DTW immediately before sampling (slimes only):. _ _,_M"""'"~.,__2\ ________ _
Weather Conditions at Time of Sampling:_..,.S....,v..""o .... o_,_,,1}rr------------
Analytical Parameters/Sample Collection Method: Do..-te 'a/2 1/2.0I~
voes ljl Yes. oNo 0 ~· t"e"!\ Metals rl Yes ONO D 1:,,
Nutrients ~Yes DNo o Yes D 0 QD
Other Non Ef, Yes oNo oYes 0 D ~ Radiolo ics 'E"ert
Gross Alpha 1J Yes oNo oYes i,:No D D ri &EL
SVOCs ~Yes oNo oYes No D 0 i:ner
Conductivity 151 Yes DNo DYes lij No D D &EL
QC Samples Associated with this Location:
o Rinsate Blank
o Duplicate
Duplicate Sample Name:
f :U' ~fe~! 0 "at t&± o gzg:. ~"C!l~:::i C.Qll~c±~J ~ Q8.35 .
Field Data Record-Tailings Solutions, LDS and Slimes Drain Sampling
Location: SI; m ~~ it-~ Sampling Personnel:,_~....!..!:);!=~=~i-!--=~~!:U'
OeA" Is this a Slimes Drain? DJ Yes o No
If this is a Slimes Drain, measure depth to wastewat~r immediately before sampling.
DTW immediately before sampling (slimes only):,~~-.....f1u.., .K.0.-0;._ _____ _
Weather Conditions at Time of Sampling:_...,.::>..:..:v..,.,.._,_o .... o~~------------
Analytical Parameters/Sample Collection Method: Do..1"e S/2.l{z.ot<t
oNo D Y~-~No D ~ 0
Metals oNo bYes r$lNo D @ 0
Nutrients DNo DYes ~No D ~ 0
Other Non i, Yes DNo oYes ijl No D s D
Radiolo ·cs
Gross Alpha Bl Yes oNo DYes BI No D Iii D
SVOCs ~ Yes DNo o Yes ll No 0 ~ 0
Conductivity L'J Yes DNo oYes C, No 0 Ill 0
QC Samples Associated with this Location:
o Rinsate Blank
o Duplicate
Duplicate Sample Name:. ___________ _
Notes: Arr:,\ed oo sa ~ at 08S9 Sgpip)e~ c.olle c..+d d\.i' O'fO S
L~.Q. ·;;+< ci~ 0111
Field Data Record-Tailings Solutions, LDS and Slimes Drain Sampling
Location: _C=-=e.=l-=-1-~.....;;._ _____ Sampling Personnel: ~!la<:c ~o 11:1~~. o~~o ~r'la."'
De."'" ltc"'a.::non M11.rti Sro..:.t\ •oM Lo.11ct..S, Is this a Slimes Drain? o Yes ~ No ' •
If this is a Slimes Drain, measure depth to wastewat~r immediately before sampling.
DTW immediately before sampling (slimes only):__._N. ..... '/'--'A_,__ _______ _
Weather Conditions at Time of Sampling:,_....,,~,,c.·· .:.:,\A.uO..a..:.0.::;,~1-------------
Analytical Parameters/Sample Collection Method: t 0 / / Oo,,.•e o 2.1 201'i
Metals 1g1 Yes oNo oYes i;, No
Nutrients oo Yes DNo oYes IJl No
Other Non !SD Yes oNo oYes ill No
Radiologies
Gross Alpha r, Yes oNo oYes Ill No
SVOCs ~ Yes ONo oYes ijj No
Conductivity Eill Yes oNo D Yes l'.i!No
QC Samples Associated with this Location:
D Rinsate Blank
D Duplicate
D D
D D
0 D
D 0
0 0
D D
Duplicate Sample Name:, ___________ _
l'il
fill
l2l
OI
liJ
Ii)
Notes: Acc i \Je J on s,-+t! 0.t 09 /lf .:><i!.n:,plcs c.olle, +cJ 6.± D<J z.o.
kc£t s.,±c. o..+ u j~
G-EL
G-'E.L -.J
Field Data Record-Tailings Solutions-, LDS and Slimes Drain Sampling
Location: ..,.Cc..;e=l'----1-~.......:....:A'------Sampling Personnel: --fo..t\nu J.Joll ,·Jo.~.Oc~n ~mo."
Oe.A.t'\ Her\de.non M.uf i Sro..:.I\ "ToM Lo.11co..s.~ Is this a Slimes Drain? o Yes ~ No 1 1
If this is a Slimes Drain, measure depth to wastewat~r immediately before sampling.
DTW immediately before sampiing (slimes only):. _ _,A.,;0;;,_;'!t...;_~---------
Weather Conditions at Time of Sampling:_""'!:>..:.. v..>Clo.U.n ..... o-::;11itJ1--------------
Analytical Parameters/Sample Collection Method: Do..-+e ~/2 1/2.0I'{
voes i,i Yes oNo o Yes $l No D D fj(l C()i"th ....
Metals IYl Yes DNo bYes m No D D ~ "I;::)
1:.nent u..
Nutrients ~Yes oNo oYes r, No D D !Sil ~ £r1ero....t
Other Non 111 Yes DNo oYes IE. No D D ........ ijl
Radiolostlcs &ier~'\
Gross Alpha rfJ Yes oNo oYes Ill No D 0 ~ &EL.-
SVOCs [:JI Yes oNo oYes ['J]No D D 111 "6-ie.ra..i
Conductivity r:I Yes DNo oYes ~No D D '¥1 "I.J
(r-,=.1
QC Samples Associated with this Location:
o Rinsate Blank
o Duplicate
Duplicate Sample Name:. ___________ _
Notes: Arr: ved on s:te u-.t 09 3 5, s l.\mp\es c ollec.ted o.+ oq YD
I C rt-s H::e. ~ -fY} 1 I 'f lD D g
Field Data Record~ Tailings Solutions, LDS and Slimes Drain Sampling
Location: Ce.\\ YA LDS Sampling Personnel: ~I\OGC ~o ll;J.,.~, Deco L,t1mo.ri
DieA." Hcn~~l"~on M"-rf i Srow(l loM La11l45.1 Is this a Slimes Drain? o Yes i, No ' •
If this is a Slimes Drain, measure depth to wastewat~r immediately before sampling.
DTW immediately before sampling (slimes only):._L.Otl,=V&}c::i.---------
Weather Conditions at Time of Sampling:_ ..... s,· v.,.""-llO.u.0~~1--------------
Analytical Parameters/Sample Collection Method: Oo,.""te <o/2.l/2.0I'{
voes ijl Yes DNo oYes
Metals MYes oNo oYes D fill
Nutrients !JI Yes DNo o Yes Iii No D D ~
Other Non ~ Yes oNo D Yes Ill No D D IS;'
Radiolo cs
Gross Alpha Yes DNo oYes No D 0 " SVOCs ~ Yes oNo oYes ~No D 0 ~
Conductivity Iii Yes oNo oYes Ill No D D ~
QC Samples Associated with thjs Location:
o Rinsate Blank
D Duplicate
Duplicate Sample Name:
Notes: Acc;11e d on Scte Le:G: .,,·te o.± tuOts
09 'iO, ~~m p}es co /Jec.+etl a.+ QC/45
Field Data Record-Tailings Solutions, LDS and Slimes Drain Sampling
Location: Ce) l L) B
Is this a Slimes Drain?
Sampling Personnel:_~.!..!!l.!Jll.!la.--1.!.!!!..!.!!!~~~~
De.Af\
D Yes r,J No
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampiing (slimes only): .... -4~~'--'-----------
Weather Conditions at Time of Sampling-:_~S"'v...,,.o .... n=~~------------
Analytical Parameters/Sample Collection Method: Do..1'e S/2.1/201<:t
voes ijJ Yes oNo
Metals ii Yes DNo
Nutrients [JI Yes oNo
Other Non 'l) Yes DNo oYes
Radiolo ·cs
Gross Alpha IJ Yes oNo oYes
SVOCs ~Yes oNo oYes No
Conductivity IJl Yes DNo DYes No
QC Samples Associated with thjs Location:
o Rinsate Blank
D Duplicate
D D
D D
D D
D D
Duplicate Sample Name:. ___________ _
Notes: Au:\led Do ~:±e Joos SCtlt'.)fles c.olleded e.+ }CJJ.5 . Lell .S([r a-+ !D2.7
G-EL
6-E:l...
Field Data Record-Tailings Solutions, LDS and Slimes Drain Sampling
Location: Ce.I I 4 3 LDS Sampling Personnel: ~aoec f.loll;J.,.~. o~0 ~mo."
Oe."'-" He"Jer~on Mo.r-fi Srowl'\ loft'\ LMc~~ Is this a Slimes Drain? o Yes Iii No ' •
If this is a Slimes Drain, measure depth to wastewat~r immediately before sampling.
DTW immediately before sampling. (slimes only):.__.Ld/,;:!.L.,/..:4......__ _______ _
Weather Conditions at Time of Sampling:_...,.,.::>..:..:\A;~Ol..ll.!..:0~~------------
Analytical Parameters/Sample Collection Method: Do..-te S/2.ljz.oi~
voes @Yes oNo DYes fiJ No 0 D 6i f=tlera 1.9
Metals ~Yes DNo bYes r, No D D ti ~(I~~
Nutrients MYes ONo o Yes CJ No D D "'-' ~ ,::::..,e('lh.l.
Other Non (fl Yes DNo oYes 1¥ No D D (Ji -·..J
Radiolocics Ener~.'-\
Gross Alpha ~ Yes DNo oYes ~No D D ~ &EL
SVOCs Iii Yes DNo o Yes l1l No D 0 .. r;w ~era.,'"'
Conductivity 111 Yes oNo oYes 11} No 0 D 00 6-t=: L
QC Samples Associated with this Location:
o Rinsate Blank
o Duplicate
Duplicate Sample Name:
Field Data Record-Tailings Solutions, LDS and Slimes Drain Sampling
Location: C e.1 I G:,5
Is this a Slimes Drain?
Sampling Personnel: ""!l~~~=-.."'-=="--"-'-~
Oe~" o Yes ijl, No
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only):_//.<..:...L../:';,:..i:r'\=----------
Weather Conditions at Time of Sampling:._"""'::>""" .. =v.. ..... l'.l"""'0-=.~11--------------
Analytical Parameters/Sample Collection Method: Oo,,.-+e <a/2.i/2.0l't
Parametef;, '· Safup.¢ :X:afcen ... -fi~~i{: ';il:4,: .. '. . .,. ~'\-< .. / .. :-·:: ... ,\,I'-.. . . , .. -" <:, , 4~. .. ··11· •' . , .. ':-. . ...
voes rA Yes oNo D Yes i, No
Metals ct! Yes oNo D Yes OONo
Nutrients ~Yes ONO oYes E1l No
Other Non IE Yes DNo oYes i, No
Radiologies
Gross Alpha Ill Yes oNo o Yes Bl No
SVOCs f$ Yes oNo oYes i,No
Conductivity ~Yes DNo o Yes SI No
QC Samples Associated with thjs Location:
o Rinsate Blank
•. · ,. · 'l-· ..... s; ~~iin ·M· boo ( .. ,t · · ~·.· , ·. '. amp_ lit . et ,_ .. ,,.··: .. ,-. . ·,
Perl taltic· ..Bailer':· , Lallie··-. .--;-' .J ••• ~-'"" ., • '•• .1:~ ·• ,. • ... -... ,-• • ,t I .. }PQnip . • ~·'
D D ~
D D ijLI
D D ~
D D Iii
D D ii
D D ~
D D ~
fj( Duplicate
Duplicate Sample Name:_--=G::;;...e=l'-'-l---=b=5=------
\
~;/Lati
~-r ,1' • .-Name
t::nen,.._. ..__,
~er111..1
Y-:,1C(l1:
Y....J
~u-e-i'\
6-E'.L
ft1tf't\lJ
6-1:=.L ,.__,
TabB
Sample Location Figures
/
·21
MW-02 •
32
MW-03 •
0 llllO'
IIW.i: 1" • 1,CIDO'
CELL 1
LEAK
DETECTION
SAMPLE
LOCATION
MW•17 •
MW-27 ...
CELL 2
33
PIEZ-2 •
PIEZ-3 •
M ·26 TW4•1 <f)T'W4-fJ
O OTW4•3 OTW4-12
OTW4•11bTW4-11 C'lW4·13
•
PIEZ-5 •
TW4-~B
OTW4•1
.. Energy Fuels Resources (USA) Inc.
Whtta Meaa MIii
San Juan : utah
T37S, R22E
Annual Talllngs System
Slimes and Leak Detection
Sample Locations
Allnllr: ----: 11 24 15
,I
I.J It,
" 1
r
i
& Ii:
l ~
,I ~
li :I .,
{
~ f i
f ;.
~ i I .,c -l f I
MW-02 •
MW-2 •
32
MW-03 •
-
CELL 1
MW-27 •
PIEZ-2 •
PIEZ-3 •
..-!:::===:f===t::::==::::::::::::~~zzt:.....=::+·rw4.20 OTW4•5
0 -_,._,patl
MW-17 •
CELL 2
33
M ·26 TW4•1 ifl1W4•9
O 01W4..J 01W4-12
PIEZ-t •
PIEZ-5 •
OTW4-4CJTW4·14
OTW4-6
~ Energy Fuels Resources (USA) Inc.
Mlar:
White Maea MUI
San Juan Utah
n: TJ7S, R22E
Annual TaDlnga System,
Cell Solution
Sample Locations
,, 2'4 15
TabC
Laboratory Analytical Reports
EN:RGY •' Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C19081073-001
Client Sample ID: Cell 1
Analyses
MAJOR IONS
Alkalinity, Total as CaC03
Carbonate as C03
Bicarbonate as HC03
Chloride
Fluoride
Sulfate
PHYSICAL PROPERTIES
Conductivity @ 25 C
pH
pH Measurement Temp
Solids, Total Dissolved TDS@ 180 C
NUTRIENTS
Nitrogen, Nitrate+Nitrite as N
Nitrogen, Ammonia as N
METALS, DISSOLVED
Arsenic
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Tin
Uranium
Vanadium
Zinc
VOLATILE ORGANIC COMPOUNDS
Tetrahydrofuran
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND mg/L
ND mg/L
ND mg/L
19800 mg/L
3480 mg/L
169000 mg/L
119000 umhos/cm
1.14 s.u.
17 oc
257000 mg/L
118 mg/L
10400 mg/L
270 mg/L
0.93 mg/L
5.4 mg/L
720 mg/L
15 mg/L
66 mg/L
1700 mg/L
9100 mg/L
22 mg/L
9200 mg/L
540 mg/L
3.7 ug/L
120 mg/L
110 mg/L
2600 mg/L
10 mg/L
0.79 mg/L
28000 mg/L
ND mg/L
0.54 mg/L
81 mg/L
1400 mg/L
550 mg/L
ND ug/L
D -RL increased due to sample matrix.
Qualifiers
D
D
D
E
H
D
D
D
H -Analysis performed past recommended holding time.
MCU
RL QCL
5
5
5
100
50
400
5
0.01
2000
0.5
1000
4
0.2
0.2
70
4
0.7
1
20
20
2
0.2
2
2
40
2
70
40
0.7
0.7
0.4
4
7
35.0
Report Date: 11 /25/19
Collection Date: 08/21/19 08:35
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
A2320 B 08/23/19 15:28 / dmb
A2320 B 08/23/19 15:28 / dmb
A2320 B 08/23/19 15:28 / dmb
E300.0 09/13/19 22:51 /ljl
A4500-F C 09/13/19 14:03 / dmb
E300.0 09/13/19 22:51 / ljl
A2510 B 08/23/19 11 :30 / kjp
A4500-H B 08/23/19 11 :30 / kjp
A4500-H B 08/23/19 11 :30 / kjp
A2540 C 08/26/19 16: 11 / kjp
E353.2 08/27/19 13:54 / dmb
E350.1 08/26/1918:03 / dmb
E200.7_8 10/29/19 01 :25 / ta-a
E200.7_8 10/29/19 01 :25 / ta-a
E200.7_8 10/29/19 01 :25 / ta-a
E200.7_8 10/29/19 01 :25 / ta-a
E200.7_8 10/29/19 01 :25 / ta-a
E200.7 _8 10/29/19 01 :25 / ta-a
E200.7 _8 10/29/19 01 :25 / ta-a
E200.7 _8 10/29/19 01 :25 I ta-a
E200.7 _8 10/29/19 01 :25 / ta-a
E200.7 _8 10/29/19 01 :25 / ta-a
E200.7 _8 10/29/19 01 :25 / ta-a
E245.1 09/09/19 19:43 / ta-a
E200.7_8 10/29/19 01 :25 / ta-a
E200.7_8 10/29/19 01 :25 / ta-a
E200.7 _8 10/29/19 01 :25 / ta-a
E200.7_8 10/29/19 01 :25 / ta-a
E200.7_8 10/29/19 01 :25 / ta-a
E200.7 _8 10/29/19 01 :25 I ta-a
E200.7 _8 10/29/1901 :25 / ta-a
E200.7_8 10/29/1901 :25 / ta-a
E200.7 _8 10/29/19 01 :25 / ta-a
E200.7_8 10/29/19 01 :25 I ta-a
E200.7_8 10/29/19 01 :25 / ta-a
SW8260B 09/03/19 14:28 / ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
E -Estimated value. Result exceeds the instrument upper
quantitation limit.
Page 5 of 172
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Billings, MT 800.735 .4489 • Casper, WY 888.235.0515
Gillette, WY 866.686. 7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 08:35
Lab ID: C19081073-001 Date Received: 08/22/19
Client Sample ID: Cell 1 Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date I By
VOLATILE ORGANIC COMPOUNDS
Acetone 28 ug/L 20 SW8260B 09/04/19 07:34 / dm
Acetonitrile 20 ug/L J 20 SW8260B 09/04/19 07:34 / dm
Acrolein ND ug/L 20 SW8260B 09/04/19 07:34 / dm
Acrylonitrile ND ug/L 20 SW8260B 09/04/19 07:34 / dm
Benzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Bromobenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Bromochloromethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Bromodichloromethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Bromoform ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Bromomethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
n-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
sec-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
tert-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Carbon disulfide 1.2 ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Carbon tetrachloride ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Chlorobenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Chlorodibromomethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Chloroethane 1.7 ug/L 1.0 SW8260B 09/04/19 07:34 / dm
2-Chloroethyl vinyl ether ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Chloroform 7.5 ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Chloromethane 2.3 ug/L 1.0 SW8260B 09/04/19 07:34 / dm
2-Chlorotoluene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
4-Chlorotoluene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1,2-Dibromo-3-chloropropane ND ug/L 2.0 SW8260B 09/04/19 07:34 / dm
1,2-Dibromoethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Dibromomethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1,2-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1,3-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1,4-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Dichlorodifluoromethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1, 1-Dichloroethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1,2-Dichloroethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1, 1-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
cis-1 ,2-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
trans-1,2-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1,2-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1,3-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
2,2-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1, 1-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
cis-1 ,3-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
trans-1,3-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Ethyl benzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Hexachlorobutadiene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
J -Estimated value. The analyte was present but less
than the reporting limit.
Page 6 of 172
EN:RGY m· Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 08:35
Lab ID: C 19081073-001 Date Received: 08/22/19
Client Sample ID: Cell 1 Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
VOLATILE ORGANIC COMPOUNDS
2-Hexanone ND ug/L 20 SW8260B 09/04/19 07:34 I dm
lodomethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
lsopropylbenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
p-lsopropyltoluene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Methyl tert-butyl ether (MTBE) ND ug/L 1.0 SW8260B 09/04/19 07:34 I dm
Methyl ethyl ketone 11 ug/L J 20 SW8260B 09/04/19 07:34 I dm
Methyl isobutyl ketone ND ug/L 20 SW8260B 09/04/19 07:34 I dm
Methylene chloride ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Naphthalene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
n-Propylbenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Styrene ND ug/L 1.0 SW8260B 09/04/19 07:34 I dm
1, 1, 1,2-Tetrachloroethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1, 1,2,2-Tetrachloroethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Tetrachloroethene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Toluene ND ug/L 1.0 SW8260B 09/04/19 07:34 I dm
1,2,3-Trichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1,2,4-Trichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 I dm
1, 1, 1-Trichloroethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1, 1,2-Trichloroethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Trichloroethene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Trichlorofluoromethane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1,2,3-Trichloropropane ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1,2,4-Trimethylbenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
1,3,5-Trimethylbenzene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Vinyl acetate ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Vinyl chloride ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
m+p-Xylenes ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
a-Xylene ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Xylenes, Total ND ug/L 1.0 SW8260B 09/04/19 07:34 / dm
Surr: 1,2-Dichloroethane-d4 124 %REC 70-130 SW8260B 09/04/19 07:34 / dm
Surr: Dibromofluoromethane 126 %REC 70-130 SW8260B 09/04/19 07:34 I dm
Surr: p-Bromofluorobenzene 92.0 %REC 70-130 SW8260B 09/04/19 07:34 / dm
Surr: Toluene-dB 84.0 %REC 70-130 SW8260B 09/04/19 07:34 I dm
SEMI-VOLATILE ORGANIC COMPOUNDS
1,2,4-Trichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
1,2-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
1,3-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
1,4-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
1-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
2,4,5-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 20:21 I ta-a
2,4,6-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
2,4-Dichlorophenol ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time. J -Estimated value. The analyte was present but less
than the reporting limit.
Page 7 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABO RA TORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 08:35
Lab ID: C19081073-001 Date Received: 08/22/19
Client Sample ID: Cell 1 Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
SEMI-VOLATILE ORGANIC COMPOUNDS
2,4-Dimethylphenol ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
2,4-Dinitrophenol ND ug/L H 50 SW8270C 09/12/19 20:21 / ta-a
2,4-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
2,6-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
2-Chloronaphthalene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
2-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
2-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
2-Nitrophenol ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
3,3 · -Dichlorobenzidine ND ug/L H 50 SW8270C 09/12/19 20:21 / ta-a
4,6-Dinitro-2-methylphenol ND ug/L H 50 SW8270C 09/12/19 20:21 / ta-a
4-Bromophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
4-Chloro-3-methylphenol ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
4-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
4-Chlorophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
4-Nitrophenol ND ug/L H 50 SW8270C 09/12/19 20:21 / ta-a
Acenaphthene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Acenaphthylene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Anthracene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Azobenzene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Benzidine ND ug/L H 100 SW8270C 09/12/19 20:21 / ta-a
Benzo(a)anthracene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Benzo( a )pyrene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Benzo(b)fluoranthene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Benzo(g,h,i)perylene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Benzo(k)fluoranthene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
bis(-2-chloroethoxy)Methane ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
bis(-2-chloroethyl)Ether ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
bis(2-chloroisopropyl)Ether ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
bis(2-ethylhexyl)Phthalate ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Butylbenzylphthalate ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Chrysene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Di-n-butyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Di-n-octyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Dibenzo(a,h)anthracene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Diethyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Dimethyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Fluoranthene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Fluorene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Hexachlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Hexachlorobutadiene ND ug/L H 30 SW8270C 09/12/19 20:21 / ta-a
Hexachlorocyclopentadiene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Hexachloroethane ND ug/L H 30 SW8270C 09/12/19 20:21 / ta-a
lndeno(1 ,2,3-cd)pyrene ND ug/L H 10 SW8270C 09/12/19 20:21 / ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time.
Page 8 of 172
EN:RGY
'' ' '
Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C19081073-001
Client Sample ID: Cell 1
Analyses
SEMI-VOLATILE ORGANIC COMPOUNDS
lsophorone
m+p-Cresols
n-Nitroso-di-n-propylamine
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
o-Cresol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Qualifiers
H
H
H
H
H
H
H
H
H
H
H
H
H
H -Analysis performed past recommended holding time.
MCU
RL QCL
10
10
10
10
10
10
10
10
50
10
10
10
20
Report Date: 11 /25/19
Collection Date: 08/21/19 08:35
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
SW8270C 09/12/19 20:21 I ta-a
SW8270C 09/12/19 20:21 I ta-a
SW8270C 09/12/19 20:21 I ta-a
SW8270C 09/12/19 20:21 I ta-a
SW8270C 09/12/19 20:21 I ta-a
SW8270C 09/12/19 20:21 I ta-a
SW8270C 09/12/19 20:21 I ta-a
SW8270C 09/12/19 20:21 I ta-a
SW8270C 09/12/19 20:21 I ta-a
SW8270C 09/12/19 20:21 I ta-a
SW8270C 09/12/19 20:21 I ta-a
SW8270C 09/12/19 20:21 / ta-a
SW8270C 09/12/19 20:21 I ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 9 of 172
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Company:
Address:
Contact:
Project:
Certificate of Analysis
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 20 I 9 Characterization ----Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Celll
488668001
Water
21-AUG-19 08:35
24-AUG-19
Client
Project:
Client ID:
Report Date: September I 7, 2019
DNMI00107
DNMI001
Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method ----
-Iazardous Waste
\.STM D 5057 Specific Gravity "As Received"
ipecific Gravity 1.15 0.010 0.100 none I VHI 08/30/19 1121 1913001
The following Analytical Methods were performed: -----------------\1 et hod ___ D_e_s~cr_ic..t'--io~n"-------_________ An=-==alyst Comments
ASTM D 5057
~otes:
;;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Column headers are defined as follows:
OF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 15 of 50 SDG: 488668 Revl
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company:
Address:
Contact:
Project:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 2019 Characterization ---------------------Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Cell l
488668001
Water
21-AUG-19 08:35
24-AUG-19
Client
Parameter Qualifier Result Uncertainty
-Iigh Rad Testing
\lphaspec Th, Liquid "As Received"
~horium-228 1380 +/-344
~horium-230 7.47E+05 +/-7380
:·horium-232 4780 +/-595
:iFPC,Total Alpha Radium, Liquid "As Received"
}ross Radium Alpha 3.26E+05 +/-2590
~ucas Cell, Ra226, liquid "As Received"
tadium-226 348 +/-28.0
J-233/234,U-235/236 and U-238 "As Received"
Jranium-233/234 28400 +/-1410
Jranium-235/236 1650 +/-395
Jranium-238 28700 +/-1420
fhe following Prep Methods were perfotmed:
\1ethod Description
}L-RAD-A-026 Laboratory Fillration
The following Analytical Methods were performed:
MDC RL
552 1.00
564 1.00
361 1.00
289 1.00
26.4 1.00
678 1.00
524 1.00
513 1.00
Analyst
Project:
Client ID:
DNMI00107
DNMIOOI
Units PF DF Analyst Date Time Batch Method
pCi/L JXB7 09/11/19 19;27 1914167
pCi/L
pCi/L
pCi/L AXM6 09/12/19 1658 1914172 2
pCi/L MXH8 09/12/19 1034 1914039 3
pCi/L JXB7 09/11/19 1927 1914171 4
pCi/L
pCi/L
Date Time Prep Batch
191234 1
\1ethod D_e~s...c.cr_i""pt'--io=ncc._ ___________________ ~A~n=a~ly.st Cqmmen~-----------
DOE EML HASL-300, Th-01-RC Modified
EPA 903.0
EPA 903.1 Modified
DOE EML HASL-300, U-02-RC Modified
;;urrogate/Tracer Recovery Test
rhorium-229 Tracer
3arium Carrier
Jranium-232 Tracer
~otes:
Alphaspec Th, Liquid "As Received"
GFPC,Total Alpha Radium, Liquid "As Received"
U-233/234,U-235/236 and U-238 "As Received"
:::ounting Uncertainty is calculated at the 68% confidence level (I-sigma).
Result Nominal Recovery%
89.5
103
78.5
Acceptable Limits
(15%-125%)
(25%-125%)
(15%-125%)
;;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Page 31 of 50 SDG: 488668 Revl
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company :
Address:
Contact:
Project:
Client Sample ID:
Sample ID:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 2019 Characterization
Cell I
488668001
Parameter Qualifier Result Uncertainty MDC
Column headers are defined as follows :
DF: Dilution Factor
DL: Detection Limit
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
RL
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 32 of 50 SDG: 488668 Revl
Project:
Client ID:
DNMI00107
DNMI001
Units PF DF Analyst Date Time Batch Method
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686. 7175 • Helena, MT 871.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-002
Client Sample ID: Cell 2 Slimes
Analyses Result Units Qualifiers
MAJOR IONS
Alkalinity, Total as CaC03 ND mg/L
Carbonate as C03 ND mg/L
Bicarbonate as HC03 ND mg/L
Chloride 3870 mg/L
Fluoride 105 mg/L
Sulfate 67000 mg/L
-H -Original analysis was done within hold time. Data is from recheck analysis.
PHYSICAL PROPERTIES
Conductivity @ 25 C
pH
pH Measurement Temp
Solids, Total Dissolved TDS @ 180 C
NUTRIENTS
Nitrogen, Nitrate+Nitrite as N
Nitrogen, Ammonia as N
METALS, DISSOLVED
Arsenic
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Tin
Uranium
Vanadium
Zinc
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
55700
3.07
16
94300
33.0
4420
23
0.28
6.5
480
2.1
54
160
3600
0.59
3700
170
ND
3.2
140
710
1.3
ND
4600
0.39
ND
29
500
850
D -RL increased due to sample matrix.
umhos/cm
s.u. oc
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ug/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
H -Analysis performed past recommended holding time.
D
DH
D
E
H
D
D
D
Report Date: 11/25/19
Collection Date: 08/21/19 09:05
DateReceived: 08/22/19
Matrix: Aqueous
MCU
RL QCL Method Analysis Date / By
5 A2320 B 08/23/19 15:31 / dmb
5 A2320 B 08/23/19 15:31 / dmb
5 A2320 B 08/23/19 15:31 / dmb
50 E300.0 09/13/19 23: 10 / ljl
50 A4500-F C 09/18/19 14:25 / dmb
200 E300.0 09/13/19 23: 10 / ljl
5 A2510 B 08/23/19 11 :34 / kjp
0.01 A4500-H B 08/23/19 11 :34 / kjp
A4500-H B 08/23/19 11 :34 / kjp
500 A2540 C 08/23/19 14:02 / kjp
0.2 E353.2 08/27/19 13:55 / dmb
1000 E350.1 08/26/19 18:04 I dmb
0.2 E200.7_8 10/26/19 06:24 / ta-a
0.01 E200.7_8 10/26/19 06:24 I ta-a
0.01 E200.7_8 10/26/19 06:24 / ta-a
5 E200.7_8 10/26/19 06:24 / ta-a
0.2 E200.7_8 10/26/19 06:24 / ta-a
0.05 E200.7_8 10/26/19 06:24 / ta-a
0.8 E200.7_8 10/26/19 06:24 I ta-a
E200.7_8 10/26/19 06:24 / ta-a
0.08 E200.7_8 10/26/19 06:24 / ta-a
E200.7 _8 10/26/19 06:24 / ta-a
0.1 E200.7 _8 10/26/19 06:24 / ta-a
0.2 E245.1 09/09/19 19:45 / ta-a
0.1 E200.7_8 10/26/19 06:24 I ta-a
1 E200.7 _8 10/26/19 06:24 / ta-a
2 E200.7 _8 10/26/19 06:24 / ta-a
0.1 E200.7 _8 10/26/19 06:24 / ta-a
0.05 E200.7 _8 10/26/19 06:24 / ta-a
2 E200.7_8 10/26/19 06:24 / ta-a
0.05 E200.7 _8 10/26/19 06:24 / ta-a
0.05 E200.7_8 10/26/19 06:24 / ta-a
0.02 E200.7_8 10/26/19 06:24 / ta-a
2 E200.7 _8 10/26/19 06:24 / ta-a
5 E200.7_8 10/26/19 06:24 / ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
E -Estimated value. Result exceeds the instrument upper
quantitation limit.
Page 10 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21 /19 09:05
Lab ID: C 19081073-002 Date Received: 08/22/19
Client Sample ID: Cell 2 Slimes Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
VOLATILE ORGANIC COMPOUNDS
Tetrahydrofuran ND ug/L 10.0 SW8260B 09/03/19 14:50 I ta-a
Acetone 449 ug/L H 200 SW8260B 09/05/19 22: 17 / dm
Acetonitrile 206 ug/L 20 SW8260B 09/04/19 08:05 I dm
Acrolein ND ug/L 20 SW8260B 09/04/19 08:05 I dm
Acrylonitrile ND ug/L 20 SW8260B 09/04/19 08:05 / dm
Benzene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Bromobenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 / dm
Bromochloromethane ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Bromodichloromethane ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Bromoform ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Bromomethane 0.86 ug/L J 1.0 SW8260B 09/04/19 08:05 / dm
n-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
sec-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
tert-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Carbon disulfide 16 ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Carbon tetrachloride ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Chlorobenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Chlorodibromomethane ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Chloroethane 6.6 ug/L 1.0 SW8260B 09/04/19 08:05 I dm
2-Chloroethyl vinyl ether ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Chloroform 16 ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Chloromethane 2.2 ug/L 1.0 SW8260B 09/04/19 08:05 I dm
2-Chlorotoluene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
4-Chlorotoluene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1 ,2-Dibromo-3-chloropropane ND ug/L 2.0 SW8260B 09/04/19 08:05 I dm
1,2-Dibromoethane ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Dibromomethane ND ug/L 1.0 SW8260B 09/04/19 08:05 / dm
1,2-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1,3-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1,4-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Dichlorodifluoromethane ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1, 1-Dichloroethane ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1,2-Dichloroethane ND ug/L 1.0 SW8260B 09/04/19 08:05 / dm
1, 1-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
cis-1,2-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
trans-1 ,2-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1 ,2-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1,3-Dichloropropane ND ug/L 1,0 SW8260B 09/04/19 08:05 I dm
2,2-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1, 1-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
cis-1,3-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
trans-1,3-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Ethylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time. J -Estimated value. The analyte was present but less
than the reporting limit.
Page 11 of 172
EI\ERGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686. 7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 09:05
Lab ID: C 19081073-002 Date Received: 08/22/19
Client Sample ID: Cell 2 Slimes Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date I By
VOLATILE ORGANIC COMPOUNDS
Hexachlorobutadiene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
2-Hexanone 11 ug/L J 20 SW8260B 09/04/19 08:05 I dm
lodomethane ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
lsopropylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 / dm
p-lsopropyltoluene ND ug/L 1.0 SW8260B 09/04/19 08:05 / dm
Methyl tert-butyl ether (MTBE) ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Methyl ethyl ketone 135 ug/L 20 SW8260B 09/04/19 08:05 I dm
Methyl isobutyl ketone 12 ug/L J 20 SW8260B 09/04/19 08:05 I dm
Methylene chloride 0.49 ug/L J 1.0 SW8260B 09/04/19 08:05 / dm
Naphthalene 13 ug/L 1.0 SW8260B 09/04/19 08:05 / dm
n-Propylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Styrene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1, 1, 1,2-Tetrachloroethane ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1, 1,2,2-Tetrachloroethane ND ug/L 1.0 SW8260B 09/04/19 08:05 / dm
Tetrachloroethene ND ug/L 1.0 SW8260B 09/04/19 08:05 / dm
Toluene 2.4 ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1,2,3-Trichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1,2,4-Trichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1, 1, 1-Trichloroethane ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1, 1,2-Trichloroethane ND ug/L 1.0 SW8260B 09/04/19 08:05 / dm
Trichloroethene ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Trichlorofluoromethane ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1,2,3-Trichloropropane ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
1,2,4-Trimethylbenzene 2.3 ug/L 1.0 SW8260B 09/04/19 08:05 / dm
1,3,5-Trimethylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:05 / dm
Vinyl acetate ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
Vinyl chloride ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
m+p-Xylenes ND ug/L 1.0 SW8260B 09/04/19 08:05 I dm
o-Xylene 0.51 ug/L J 1.0 SW8260B 09/04/19 08:05 / dm
Xylenes, Total 0.51 ug/L J 1.0 SW8260B 09/04/19 08:05 I dm
Surr: 1,2-Dichloroethane-d4 130 %REC 70-130 SW8260B 09/04/19 08:05 I dm
Surr: Dibromofluoromethane 120 %REC 70-130 SW8260B 09/04/19 08:05 I dm
Surr: p-Bromofluorobenzene 93.0 %REC 70-130 SW8260B 09/04/19 08:05 / dm
Surr: Toluene-dB 86.0 %REC 70-130 SW8260B 09/04/19 08:05 I dm
-Hold time was exceeded due to Laboratory error.
SEMI-VOLATILE ORGANIC COMPOUNDS
1,2,4-Trichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:51 I ta-a
1,2-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:51 I ta-a
1,3-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:51 I ta-a
1,4-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
1-Methylnaphthalene 12 ug/L H 10 SW8270C 09/12/19 20:51 I ta-a
2,4,5-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 20:51 I ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time. J -Estimated value. The analyte was present but less
than the reporting limit.
Page 12 of 172
EI\ERGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686. 7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 09:05
Lab ID: C 19081073-002 Date Received: 08/22/19
Client Sample ID: Cell 2 Slimes Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date I By
SEMI-VOLATILE ORGANIC COMPOUNDS
2,4,6-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
2,4-Dichlorophenol ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
2,4-Dimethylphenol ND ug/L H 10 SW8270C 09/12/19 20: 51 / ta-a
2,4-Dinitrophenol ND ug/L H 50 SW8270C 09/12/19 20:51 / ta-a
2,4-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
2,6-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
2-Chloronaphthalene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
2-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
2-Methylnaphthalene 11 ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
2-Nitrophenol ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
3,3 · -Dichlorobenzidine ND ug/L H 46 SW8270C 09/12/19 20:51 / ta-a
4,6-Dinitro-2-methylphenol ND ug/L H 50 SW8270C 09/12/19 20:51 / ta-a
4-Bromophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
4-Chloro-3-methylphenol ND ug/L H 10 SW8270C 09/12119 20:51 / ta-a
4-Chlorophenol ND ug/L H 10 SW8270C 09112/19 20:51 / ta-a
4-Chlorophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 20:51 I ta-a
4-Nitrophenol ND ug/L H 50 SW8270C 09/12/19 20:51 / ta-a
Acenaphthene ND ug/L H 10 SW8270C 09/12119 20:51 / ta-a
Acenaphthylene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Anthracene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Azobenzene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Benzidine ND ug/L H 92 SW8270C 09/12/19 20:51 / ta-a
Benzo(a)anthracene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Benzo(a)pyrene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Benzo(b)fluoranthene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Benzo(g, h, i)perylene ND ug/L H 10 SW8270C 09/12119 20:51 / ta-a
Benzo(k)fluoranthene ND ug/L H 10 SW8270C 09112/19 20:51 / ta-a
bis(-2-chloroethoxy)Methane ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
bis(-2-ch loroethyl)Ether ND ug/L H 10 SW8270C 09/12119 20:51 / ta-a
bis(2-chloroisopropyl)Ether ND ug/L H 10 SW8270C 09/12/19 20:511 ta-a
bis(2-ethylhexyl)Phthalate 1.1 ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Butylbenzylphthalate ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Chrysene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Di-n-butyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Di-n-octyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Dibenzo(a,h)anthracene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Diethyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Dimethyl phthalate 1.5 ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Fluoranthene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Fluorene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Hexachlorobenzene ND ug/L H 10 SW8270C 09112/19 20:51 / ta-a
Hexachlorobutadiene ND ug/L H 28 SW8270C 09/12/19 20:51 / ta-a
Hexachlorocyclopentadiene ND ug/L H 10 SW8270C 09/12/19 20:51 / ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time.
Page 13 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686. 7175 • Helena, MT 877 .472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-002
Client Sample ID: Cell 2 Slimes
Analyses
SEMI-VOLATILE ORGANIC COMPOUNDS
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorone
m+p-Cresols
n-Nitroso-di-n-propylamine
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
o-Cresol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
5.3 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Qualifiers
H
H
H
H
H
H
H
H
H
H
H
H
H
H
H
H -Analysis performed past recommended holding time.
MCU
RL QCL
28
10
10
10
10
10
10
10
10
10
50
10
10
10
18
Report Date: 11 /25/19
Collection Date: 08/21/19 09:05
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
SW8270C 09/12/19 20:51 / ta-a
SW8270C 09/12/19 20:51 / ta-a
SW8270C 09/12/19 20:51 / ta-a
SW8270C 09/12/19 20:51 / ta-a
SW8270C 09/12/19 20:51 / ta-a
SW8270C 09/12/19 20:51 / ta-a
SW8270C 09/12/19 20:51 / ta-a
SW8270C 09/12/19 20:51 / ta-a
SW8270C 09/12/19 20:51 / ta-a
SW8270C 09/12/19 20:51 I ta-a
SW8270C 09/12/19 20:51 / ta-a
SW8270C 09/12/19 20:51 / ta-a
SW8270C 09/12/19 20:51 I ta-a
SW8270C 09/12/19 20:51 I ta-a
SW8270C 09/12/19 20:51 / ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 14 of 172
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company:
Address:
Contact:
Project:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 2019 Characterization ----------------Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Cell 2 Slimes
488668002
Water
21-AUG-19 09:05
24-AUG-19
Client
Parameter Qualifier Result ----------Iazardous Waste
\STM D 5057 Specific Gravity "As Received"
,pecific Gravity 1.03
The following Analytical Methods were performed:
\.1ethod Descri tion
ASTMD 5057
lilotes:
DL RL
0.010 0.100
Project:
Client ID:
DNMI00107
DNMI001
Units PF DF Analyst Date Time Batch Method
none I VHI 08/30/19 1123 1913001
Anal st Comments~-----~
,RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 16 of 50 SDG: 488668 Revl
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company:
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Contact:
Lakewood, Colorado 80228
Ms. Kathy Weinel
Project: Tailings 2019 Characterization
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Cell 2 Slimes
488668002
Water
21-AUG-19 09:05
24-AUG-19
Client
Parameter Qualifier Result Uncertainty
-Iigh Rad Testing
\lphaspec Th, Liquid "As Received"
:horium-228 u 3.58 +/-128
:horium-230 1750 +/-362
.'horium-232 u -36.3 +/-72.3
}FPC,Total Alpha Radium, Liquid "As Received"
]ross Radium Alpha 3790 +/-302
~ucas Cell, Ra226, liquid "As Received"
tadium-226 62.5 +/-13.5
J-233/234,U-235/236 and U-238 "As Received"
Jranium-233/234 9300 +/-789
Jranium-235/236 484 +/-214
Jranium-238 9150 +/-781
fhe following Prep Methods were performed:
Vlethod Description
JL-RAD-A-026 Laboratory Filtration
The following Analytical Methods were performed:
\11.ethod Descri tion
DOE EML HASL-300, Th-01-RC Modified
EPA 903.0
EPA 903.1 Modified
DOE EML HASL-300, U-02-RC Modified
iurrogatel'Tracer Recovery Test
Alphaspcc Th, Liquid "As Re ceived"
MDC
553
523
378
200
24.0
555
242
505
rhorium-229 Tracer
3arium Carrier
Jranium-232 Tracer
GFPC,Total Alpha Radium Liquid "As Received"
U-233/234,U-235/236 and U-238 "As Received"
\Jotes:
RL
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Analyst
:::ounting Uncertainty is calculated at the 68% confidence level (I-sigma).
Project:
Client ID:
DNMI00107
DNMI001
Units PF DF Analyst Date Time Batch Method
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
Date
Result
JXB7 09/11/19 1927 1914167
AXM6 09/12/19 1658 1914172 2
MXH8 09/12/19 1034 1914039 3
JXB7 09/11/1 9 1927 1914171 4
Time Prep Batch
1912341
Anal st Comments
Nominal Recovery%
86.9
101
86.7
Acceptable Limits
(15%-125%)
(25%-125%)
(15%-125%)
iRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Page 33 of 50 SDG: 488668 Revl
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Company :
Address:
Contact:
Project:
Client Sample ID:
Sample ID:
Certificate of Analysis
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 2019 Characterization ------Cell 2 Slimes
488668002
Project:
Client ID:
Report Date: September 17, 2019
DNMI00107
DNMIOOl
Parameter Qualifier Result Uncertainty __ M_D_C ___ RL ____ Units PF DF Analyst Date Time Batch Method
Column headers are defined as follows:
OF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 34 of 50 SDG: 488668 Revl
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
EI\ERGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-003
Client Sample ID: Cell 3
Analyses Result Units Qualifiers
MAJOR IONS
Alkalinity, Total as CaC03 ND mg/L
Carbonate as C03 ND mg/L
Bicarbonate as HC03 ND mg/L
Chloride 15000 mg/L D
Fluoride 1340 mg/L D
Sulfate 96000 mg/L D
PHYSICAL PROPERTIES
Conductivity @ 25 C 95500 umhos/cm E
pH 3.88 s.u. H
pH Measurement Temp 17 oc
Solids, Total Dissolved TDS@ 180 C 143000 mg/L D
NUTRIENTS
Nitrogen, Nitrate+Nitrite as N 925 mg/L D
Nitrogen, Ammonia as N 9000 mg/L D
METALS, DISSOLVED
Arsenic 0.38 mg/L
Beryllium 0.35 mg/L
Cadmium 7.4 mg/L
Calcium 510 mg/L
Chromium 0.23 mg/L
Cobalt 64 mg/L
Copper 35 mg/L
Iron 2500 mg/L
Lead ND mg/L
Magnesium 10000 mg/L
Manganese 1000 mg/L
Mercury 0.20 ug/L
Molybdenum 0.55 mg/L
Nickel 150 mg/L
Potassium 630 mg/L
Selenium 2.9 mg/L
Silver 0. 11 mg/L
Sodium 14000 mg/L
Thallium 0.17 mg/L
Tin ND mg/L
Uranium 19 mg/L
Vanadium 54 mg/L
Zinc 950 mg/L
VOLATILE ORGANIC COMPOUNDS
Tetrahydrofuran ND ug/L
Report RL -Analyte reporting limit.
Definitions: QCL -Quality control limit.
D -RL increased due to sample matrix.
H -Analysis performed past recommended holding time.
MCU
RL QCL
5
5
5
100
50
400
5
0.01
1000
5
1000
0.2
0. 1
0.01
5
0.2
0.05
0.08
0.08
0.1
0.2
0.1
1
2
0.1
0.05
20
0.05
0.05
0.02
0.2
5
35.0
Report Date: 11 /25/19
Collection Date: 08/21/19 09:20
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
A2320 B 08/23/19 15:34 / dmb
A2320 B 08/23/19 15:34 / dmb
A2320 B 08/23/19 15:34 / dmb
E300.0 09/10/19 13:30 / ljl
A4500-F C 08/26/19 18:25 / dmb
E300.0 09/10/19 13:30 / ljl
A2510 B 08/23/19 11 :40 / kjp
A4500-H B 08/23/19 11 :40 / kjp
A4500-H B 08/23/19 11 :40 / kjp
A2540 C 08/23/19 14:03 / kjp
E353.2 08/27/19 13:56 / dmb
E350.1 08/26/19 18:05 / dmb
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E245.1 09/09/19 14:44 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
E200.7 _8 10/26/19 06:31 / ta-a
SW8260B 09/03/19 15: 11 / ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
E -Estimated value. Result exceeds the instrument upper
quantitation limit.
Page 15 of 172
EN:RGY
' '
Trust our People. Trust our Data.
www energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 09:20
Lab ID: C 19081073-003 Date Received: 08/22/19
Client Sample ID: Cell 3 Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
VOLATILE ORGANIC COMPOUNDS
Acetone 135 ug/L 20 SW8260B 09/04/19 08:37 / dm
Acetonitrile ND ug/L 20 SW8260B 09/04/19 08:37 / dm
Acrolein ND ug/L 20 SW8260B 09/04/19 08:37 / dm
Acrylonitrile ND ug/L 20 SW8260B 09/04/19 08:37 / dm
Benzene ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
Bromobenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
Bromochloromethane ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
Bromodichloromethane ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Bromoform ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
Bromomethane ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
n-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
sec-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
tert-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Carbon disulfide 0.84 ug/L J 1.0 SW8260B 09/04/19 08:37 / dm
Carbon tetrachloride ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
Chlorobenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
Chlorodibromomethane ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Chloroethane 1.9 ug/L 1.0 SW8260B 09/04/19 08:37 / dm
2-Chloroethyl vinyl ether ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
Chloroform 18 ug/L 1.0 SW8260B 09/04/19 08:37 / dm
Chloromethane 2.8 ug/L 1.0 SW8260B 09/04/19 08:37 / dm
2-Chlorotoluene ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
4-Chlorotoluene ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
1,2-Dibromo-3-chloropropane ND ug/L 2.0 SW8260B 09/04/19 08:37 I dm
1,2-Dibromoethane ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
Dibromomethane ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
1,2-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
1,3-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1,4-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Dichlorodifluoromethane ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
1, 1-Dichloroethane ND ug/L 1.0 SW8260B 09/04/19 08:37 / dm
1,2-Dichloroethane ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1 , 1-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
cis-1,2-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
trans-1 ,2-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1,2-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1,3-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
2,2-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1, 1-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
cis-1 ,3-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
trans-1 , 3-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Ethylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Hexachlorobutadiene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
J -Estimated value. The analyte was present but less
than the reporting limit.
Page 16 of 172
EN:RGY
I , ,
Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21 /19 09:20
Lab ID: C 19081073-003 DateReceived: 08/22/19
Client Sample ID: Cell 3 Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
VOLATILE ORGANIC COMPOUNDS
2-Hexanone 5.0 ug/L J 20 SW8260B 09/04/19 08:37 I dm
lodomethane ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
lsopropylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
p-lsopropyltoluene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Methyl tert-butyl ether (MTBE) ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Methyl ethyl ketone 34 ug/L 20 SW8260B 09/04/19 08:37 I dm
Methyl isobutyl ketone ND ug/L 20 SW8260B 09/04/19 08:37 I dm
Methylene chloride 0.67 ug/L J 1.0 SW8260B 09/04/19 08:37 I dm
Naphthalene 0.57 ug/L J 1.0 SW8260B 09/04/19 08:37 I dm
n-Propylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Styrene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1, 1, 1,2-Tetrachloroethane ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1, 1,2,2-Tetrachloroethane ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Tetrachloroethene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Toluene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1,2,3-Trichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1,2,4-Trichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1, 1, 1-Trichloroethane ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1, 1,2-Trichloroethane ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Trichloroethene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Trichlorofluoromethane ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1,2,3-Trichloropropane ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1,2,4-Trimethylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
1,3,5-Trimethylbenzene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Vinyl acetate ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Vinyl chloride ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
m+p-Xylenes ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
a-Xylene ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Xylenes, Total ND ug/L 1.0 SW8260B 09/04/19 08:37 I dm
Surr: 1,2-Dichloroethane-d4 120 %REC 70-130 SW8260B 09/04/19 08:37 I dm
Surr: Dibromofluoromethane 122 %REC 70-130 SW8260B 09/04/19 08:37 I dm
Surr: p-Bromofluorobenzene 92.0 %REC 70-130 SW8260B 09/04/19 08:37 I dm
Surr: Toluene-dB 84.0 %REC 70-130 SW8260B 09/04/19 08:37 I dm
SEMI-VOLATILE ORGANIC COMPOUNDS
1,2,4-Trichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:20 / ta-a
1,2-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
1,3-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
1,4-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
1-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
2,4,5-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 20:20 / ta-a
2,4,6-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
2,4-Dichlorophenol ND ug/L H 10 SW8270C 09/12/19 20:20 / ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time. J -Estimated value. The analyte was present but less
than the reporting limit.
Page 17 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 09:20
Lab ID: C 19081073-003 Date Received: 08/22/19
Client Sample ID: Cell 3 Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
SEMI-VOLATILE ORGANIC COMPOUNDS
2,4-Dimethylphenol ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
2,4-Dinitrophenol ND ug/L H 50 SW8270C 09/12/19 20:20 I ta-a
2,4-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
2,6-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
2-Chloronaphthalene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
2-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
2-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
2-Nitrophenol ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
3,3 · -Dichlorobenzidine ND ug/L H 45 SW8270C 09/12/19 20:20 I ta-a
4,6-Dinitro-2-methylphenol ND ug/L H 50 SWB270C 09/12/19 20:20 I ta-a
4-Bromophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
4-Chloro-3-methylphenol ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
4-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
4-Chlorophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
4-Nitrophenol ND ug/L H 50 SW8270C 09/12/19 20:20 I ta-a
Acenaphthene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Acenaphthylene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Anthracene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Azobenzene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Benzidine ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Benzo(a)anthracene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Benzo(a)pyrene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Benzo(b)fluoranthene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Benzo(g,h,i)perylene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Benzo(k)fluoranthene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
bis(-2-chloroethoxy)Methane ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
bis(-2-chloroethyl)Ether ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
bis(2-chloroisopropyl)Ether ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
bis(2-ethylhexyl)Phthalate ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Butylbenzylphthalate ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Chrysene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Di-n-butyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Di-n-octyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Dibenzo(a,h)anthracene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Diethyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Dimethyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Fluoranthene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Fluorene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Hexachlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Hexachlorobutadiene ND ug/L H 27 SW8270C 09/12/19 20:20 I ta-a
Hexachlorocyclopentadiene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Hexachloroethane ND ug/L H 27 SW8270C 09/12/19 20:20 I ta-a
lndeno(1,2,3-cd)pyrene ND ug/L H 10 SW8270C 09/12/19 20:20 I ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time.
Page 18 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-003
Client Sample ID: Cell 3
Analyses
SEMI-VOLATILE ORGANIC COMPOUNDS
lsophorone
m+p-Cresols
n-Nitroso-di-n-propylamine
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
o-Cresol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Qualifiers
H
H
H
H
H
H
H
H
H
H
H
H
H
H -Analysis performed past recommended holding time.
MCU
RL QCL
10
10
10
10
10
10
10
10
50
10
10
10
18
Report Date: 11 /25/19
Collection Date: 08/21/19 09:20
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date I By
SW8270C 09/12/19 20:20 I ta-a
SW8270C 09/12/19 20:20 I ta-a
SW8270C 09/12/19 20:20 I ta-a
SW8270C 09/12/19 20:20 I ta-a
SW8270C 09/12/19 20:20 I ta-a
SW8270C 09/12/19 20:20 I ta-a
SW8270C 09/12/19 20:20 I ta-a
SW8270C 09/12/19 20:20 I ta-a
SW8270C 09/12/19 20:20 I ta-a
SW8270C 09/12/19 20:20 I ta-a
SW8270C 09/12/19 20:20 I ta-a
SW8270C 09/12/19 20:20 / ta-a
SW8270C 09/12/19 20:20 / ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 19 of 172
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Contact: Ms. Kathy Weinel
Project: Tailings 2019 Characterization ------------------
Client Sample ID: Cell 3
Sample ID: 488668003
Matrix: Water
Collect Date: 21-AUG-19 09:20
Receive Date: 24-AUG-19
Collector: Client
Parameter Qualifier Result DL RL -------------------
-Iazardous Waste
\STM D 5057 Specific Gravity "As Received"
ipecific Gravity 1.07 0.010 0.100
The following Analytical Methods were perform_e_d_: ____ _
Project:
Client ID:
DNMI00107
DNMI001
Units PF DF Analyst Date Time Batch Method
none I VHI 08/30/19 1124 1913001
·=\.1=et=h=o=d _____ --=D:....:e=s=crcc.Jip=t""io:..;.;n;__ __________________ ...,A=n~yst Comments _________ _
ASTMD 5057
~otes:
iRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Column headers are defined as follows:
OF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 17 of 50 SDG: 488668 Revl
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company:
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Contact: Ms. Kathy Weinel
Project: Tailings 2019 Characterization --------------------------Client Sample ID: Cell 3 Project:
Sample ID: 488668003 Client ID:
Matrix: Water
Collect Date: 21-AUG-19 09:20
Receive Date: 24-AUG-19
Collector: Client
DNMI00107
DNMI001
Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method
-Iigh Rad Testing
\lphaspec Th, Liquid "As Received"
'horium-228 u 196
:horium-230 6610
:horium-232 u 222
:iFPC,Total Alpha Radium, Liquid "As Received"
}ross Radium Alpha 3890
~ucas Cell, Ra226, liquid "As Received"
{adium-226 48.0
J-233/234,U-235/236 and U-238 "As Received"
Jranium-233/234 6640
Jranium-235/236 u 109
Jranium-238 5780
[he following Prep Methods were performed:
+/-179 573
+/-724 675
+/-152 286
+/-302 186
+/-13.1 32.9
+/-781 670
+/-156 327
+/-723 489
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
JXB7 09/11/19 1927 1914167
AXM6 09/12/19 1658 1914172
MXH8 09/12/19 1034 1914039
JXB7 09/12/19 1204 1914171
v1ethod Description Analyst Date Time Prep Batch
--:;L---RA-D---A·--0~2-6 _____ L_a_bo'-r-at..,_ory-F~ilt-ra-ti-on-------------=------------1912341
The following Analytical Methods were performed:
2
3
4
\1ethod Descri tion ----------------~A=n=alyst Co=m=m=e=n=ts~----------
DOE EML HASL-300, Th-01-RC Modified
EPA 903.0
EPA 903.1 Modified
DOE EML HASL-300, U-02-RC Modified
;urrogate/Tracer Recovery Test
fhorium-229 Tracer
3arium Carrier
Jranium-232 Tracer
'fotes:
Alphaspec Th, Liquid "As Received"
GFPC,Total Alpha Radium, Liquid "As Received"
U-233/234,U-235/236 and U-238 "As Received"
::ounting Uncertainty is calculated at the 68% confidence level (I-sigma).
Result Nominal Recovery%
72.9
101
78.2
Acceptable Limits
(15%-125%)
(25%-125%)
(15%-125%)
;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Page 35 of 50 SDG: 488668 Revl
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Company:
Address:
Certificate of Analysis
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Contact: Ms. Kathy Weinel
Project: Tailings 2019 Characterization --------------------------Client Sample ID: Cell 3 Project:
Sample ID: 488668003 Client ID:
Report Date: September 17, 2019
DNMI00107
DNMI001
Qualifier Result Uncertainty ---------------'---------Parameter MDC RL Units PF DF Analyst Date Time Batch Method
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 36 of 50 SDG: 488668 Revl
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
EN:RGY Trust our People. Trust our Data.
www energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-004
Client Sample ID: Cell 4A
Analyses Result Units Qualifiers
MAJOR IONS
Alkalinity, Total as CaC03 ND mg/L
Carbonate as C03 ND mg/L
Bicarbonate as HC03 ND mg/L
Chloride 8670 mg/L D
Fluoride 1650 mg/L D
Sulfate 81300 mg/L D
PHYSICAL PROPERTIES
Conductivity @ 25 C 81400 umhos/cm E
pH 2.40 s.u. H
pH Measurement Temp 17 oc
Solids, Total Dissolved TDS @ 180 C 122000 mg/L D
NUTRIENTS
Nitrogen, Nitrate+Nitrite as N 70.4 mg/L D
Nitrogen, Ammonia as N 6700 mg/L D
METALS, DISSOLVED
Arsenic 63 mg/L
Beryllium 0.42 mg/L
Cadmium 2.5 mg/L
Calcium 510 mg/L
Chromium 7.2 mg/L
Cobalt 28 mg/L
Copper 580 mg/L
Iron 3200 mg/L
Lead 9.0 mg/L
Magnesium 4100 mg/L
Manganese 210 mg/L
Mercury 2.1 ug/L
Molybdenum 19 mg/L
Nickel 50 mg/L
Potassium 1200 mg/L
Selenium 3.7 mg/L
Silver 0.31 mg/L
Sodium 15000 mg/L
Thallium 0.09 mg/L
Tin 0.077 mg/L
Uranium 35 mg/L
Vanadium 150 mg/L
Zinc 280 mg/L
VOLATILE ORGANIC COMPOUNDS
Tetrahydrofuran ND ug/L
Report RL -Analyte reporting limit.
Definitions: QCL -Quality control limit.
D -RL increased due to sample matrix.
H -Analysis performed past recommended holding time.
MCU
RL QCL
5
5
5
100
50
400
5
0.01
1000
0.2
1000
0.2
0.01
0.01
50
2
0.05
0.8
0.08
10
0.1
0.2
0.1
0.1
20
0.1
0.05
20
0.05
0.05
0.02
2
5
35.0
Report Date: 11 /25/19
Collection Date: 08/21/19 09:40
Date Received: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
A2320 B 08/23/19 15:37 / dmb
A2320 B 08/23/19 15:37 / dmb
A2320 B 08/23/19 15:37 / dmb
E300.0 09/10/19 13:50 / ljl
A4500-F C 08/26/19 18:35 / dmb
E300.0 09/10/19 13:50 / ljl
A2510 B 08/23/19 11 :43 / kjp
A4500-H B 08/23/19 11 :43 / kjp
A4500-H B 08/23/19 11 :43 / kjp
A2540 C 08/23/19 14:03 / kjp
E353.2 08/27/19 12:11 / dmb
E350.1 08/26/19 18:07 / dmb
E200.7_8 10/26/19 06:37 I ta-a
E200.7 _8 10/26/19 06:37 I ta-a
E200.7_8 10/26/19 06:37 I ta-a
E200.7_8 10/26/19 06:37 / ta-a
E200.7_8 10/26/19 06:37 I ta-a
E200.7_8 10/26/19 06:37 I ta-a
E200.7 _8 10/26/19 06:37 I ta-a
E200.7_8 10/26/19 06:37 I ta-a
E200.7_8 10/26/19 06:37 I ta-a
E200.7_8 10/26/19 06:37 I ta-a
E200.7_8 10/26/19 06:37 I ta-a
E245.1 09/09/19 19:50 I ta-a
E200.7_8 10/26/19 06:37 / ta-a
E200.7_8 10/26/19 06:37 I ta-a
E200.7_8 10/26/19 06:37 I ta-a
E200.7_8 10/26/19 06:37 I ta-a
E200.7_8 10/26/19 06:37 I ta-a
E200.7 _8 10/26/19 06:37 I ta-a
E200.7 _8 10/26/19 06:37 / ta-a
E200.7 _8 10/26/19 06:37 I ta-a
E200.7 _8 10/26/19 06:37 / ta-a
E200.7 _8 10/26/19 06:37 /ta-a
E200.7_8 10/26/19 06:37 I ta-a
SW8260B 09/03/19 15:32 / ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
E -Estimated value. Result exceeds the instrument upper
quantitation limit.
J -Estimated value. The analyte was present but less
than the reporting limit.
Page 20 of 172
EI\ERCiY Trust our People. Trust our Data.
www.en~rgylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-004
Client Sample ID: Cell 4A
Analyses Result Units Qualifiers
VOLATILE ORGANIC COMPOUNDS
Acetone 39 ug/L J
Acetonitrile 21 ug/L J
Acrolein ND ug/L
Acrylonitrile ND ug/L
Benzene ND ug/L
Bromobenzene ND ug/L
Bromochloromethane ND ug/L
Bromodichloromethane ND ug/L
Bromoform ND ug/L
Bromomethane ND ug/L
n-Butylbenzene ND ug/L
sec-Butylbenzene ND ug/L
tert-Butylbenzene ND ug/L
Carbon disulfide ND ug/L
Carbon tetrachloride ND ug/L
Chlorobenzene ND ug/L
Chlorodibromomethane ND ug/L
Chloroethane 2.4 ug/L J
2-Chloroethyl vinyl ether ND ug/L
Chloroform 1.9 ug/L J
Chloromethane 1.7 ug/L J
2-Chlorotoluene ND ug/L
4-Chlorotoluene ND ug/L
1,2-Dibromo-3-chloropropane ND ug/L
1,2-Dibromoethane ND ug/L
Dibromomethane ND ug/L
1,2-Dichlorobenzene ND ug/L
1,3-Dichlorobenzene ND ug/L
1,4-Dichlorobenzene ND ug/L
Dichlorodifluoromethane ND ug/L
1, 1-Dichloroethane ND ug/L
1,2-Dichloroethane ND ug/L
1, 1-Dichloroethene ND ug/L
cis-1,2-Dichloroethene ND ug/L
trans-1,2-Dichloroethene ND ug/L
1,2-Dichloropropane ND ug/L
1,3-Dichloropropane ND ug/L
2,2-Dichloropropane ND ug/L
1, 1-Dichloropropene ND ug/L
cis-1,3-Dichloropropene ND ug/L
trans-1 ,3-Dichloropropene ND ug/L
Ethylbenzene ND ug/L
Hexachlorobutadiene ND ug/L
Report RL -Analyte reporting limit.
Definitions: QCL -Quality control limit.
J -Estimated value. The analyte was present but less
than the reporting limit.
MCU
RL QCL
50
50
50
50
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
5.0
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
Report Date: 11 /25/19
Collection Date: 08/21/19 09:40
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
SW8260B 09/04/19 09:09 / dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 / dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 / dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 / dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 / dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 / dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
SW8260B 09/04/19 09:09 I dm
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 21 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 09:40
Lab ID: C19081073-004 Date Received: 08/22/19
Client Sample ID: Cell4A Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
VOLATILE ORGANIC COMPOUNDS
2-Hexanone ND ug/L 50 SW8260B 09/04/19 09:09 I dm
lodomethane ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
lsopropylbenzene ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
p-lsopropyltoluene ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
Methyl tert-butyl ether (MTBE) ND ug/L 2.5 SW8260B 09/04/19 09:09 / dm
Methyl ethyl ketone 13 ug/L J 50 SW8260B 09/04/19 09:09 I dm
Methyl isobutyl ketone ND ug/L 50 SW8260B 09/04/19 09:09 I dm
Methylene chloride ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
Naphthalene ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
n-Propylbenzene ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
Styrene ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
1, 1, 1,2-Tetrachloroethane ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
1, 1,2,2-Tetrachloroethane ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
Tetrachloroethene ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
Toluene ND ug/L 2.5 SW8260B 09/04/19 09:09 / dm
1,2,3-Trichlorobenzene ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
1,2,4-Trichlorobenzene ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
1, 1, 1-Trichloroethane ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
1, 1,2-Trichloroethane ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
Trichloroethene ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
Trichlorofluoromethane ND ug/L 2.5 SW8260B 09/04/19 09:09 / dm
1,2,3-Trichloropropane ND ug/L 2.5 SW8260B 09/04/19 09:09 / dm
1,2,4-Trimethylbenzene ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
1,3,5-Trimethylbenzene ND ug/L 2.5 SW8260B 09/04/19 09:09 / dm
Vinyl acetate ND ug/L 2.5 SW8260B 09/04/19 09:09 / dm
Vinyl chloride ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
m+p-Xylenes ND ug/L 2.5 SW8260B 09/04/19 09:09 / dm
a-Xylene ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
Xylenes, Total ND ug/L 2.5 SW8260B 09/04/19 09:09 I dm
Surr: 1,2-Dichloroethane-d4 119 %REC 70-130 SW8260B 09/04/19 09:09 / dm
Surr: Dibromofluoromethane 108 %REC 70-130 SW8260B 09/04/19 09:09 I dm
Surr: p-Bromofluorobenzene 86.0 %REC 70-130 SW8260B 09/04/19 09:09 I dm
Surr: Toluene-dB 84.0 %REC 70-130 SW8260B 09/04/19 09:09 / dm
SEMI-VOLATILE ORGANIC COMPOUNDS
1,2,4-Trichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:49 / ta-a
1,2-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:49 / ta-a
1,3-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
1,4-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:49 / ta-a
1-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
2,4, 5-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
2,4,6-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
2,4-Dichlorophenol ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time. J -Estimated value. The analyte was present but less
than the reporting limit.
Page 22 of 172
EN:RGY
'
Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABO RA TORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21 /19 09:40
Lab ID: C19081073-004 DateReceived: 08/22/19
Client Sample ID: Cell4A Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
SEMI-VOLATILE ORGANIC COMPOUNDS
2,4-Dimethylphenol ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
2,4-Dinitrophenol ND ug/L H 50 SW8270C 09/12/19 20:49 I ta-a
2,4-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
2,6-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 20:49 / ta-a
2-Chloronaphthalene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
2-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
2-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
2-Nitrophenol ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
3,3 · -Dichlorobenzidine ND ug/L H 46 SW8270C 09/12/19 20:49 I ta-a
4,6-Dinitro-2-methylphenol ND ug/L H 50 SW8270C 09/12/19 20:49 I ta-a
4-Bromophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
4-Chloro-3-methylphenol ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
4-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
4-Chlorophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
4-Nitrophenol ND ug/L H 50 SW8270C 09/12/19 20:49 I ta-a
Acenaphthene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Acenaphthylene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Anthracene 1.2 ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Azobenzene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Benzidine ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Benzo(a)anthracene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Benzo(a)pyrene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Benzo(b )fluoranthene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Benzo(g, h, i)perylene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Benzo(k)fluoranthene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
bis(-2-chloroethoxy)Methane ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
bis(-2-ch loroethyl)Ether ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
bis(2-chloroisopropyl)Ether ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
bis(2-ethylhexyl)Phthalate ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Butylbenzylphthalate ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Chrysene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Di-n-butyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Di-n-octyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Dibenzo(a,h)anthracene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Diethyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Dimethyl phthalate ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Fluoranthene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Fluorene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Hexachlorobenzene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Hexachlorobutadiene ND ug/L H 28 SW8270C 09/12/19 20:49 I ta-a
Hexachlorocyclopentadiene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Hexachloroethane ND ug/L H 28 SW8270C 09/12/19 20:49 I ta-a
lndeno(1,2,3-cd)pyrene ND ug/L H 10 SW8270C 09/12/19 20:49 I ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time.
Page 23 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANAL YT I CAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-004
Client Sample ID: Cell 4A
Analyses
SEMI-VOLATILE ORGANIC COMPOUNDS
lsophorone
m+p-Cresols
n-Nitroso-di-n-propylamine
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
o-Cresol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Qualifiers
H
H
H
H
H
H
H
H
H
H
H
H
H
H -Analysis performed past recommended holding time.
MCU
RL QCL
10
10
10
10
10
10
10
10
50
10
10
10
19
Report Date: 11 /25/19
Collection Date: 08/21/19 09:40
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
SW8270C 09/12/19 20:49 / ta-a
SW8270C 09/12/19 20:49 / ta-a
SW8270C 09/12/19 20:49 I ta-a
SW8270C 09/12/19 20:49 / ta-a
SW8270C 09/12/19 20:49 I ta-a
SW8270C 09/12/19 20:49 / ta-a
SW8270C 09/12/19 20:49 I ta-a
SW8270C 09/12/19 20:49 I ta-a
SW8270C 09/12/19 20:49 I ta-a
SW8270C 09/12/19 20:49 I ta-a
SW8270C 09/12/19 20:49 / ta-a
SW8270C 09/12/19 20:49 I ta-a
SW8270C 09/12/19 20:49 I ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 24 of 172
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Company :
Address:
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Certificate of Analysis
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 2019 Characterization
Ce114 A
488668004
Water
21-AUG-19 09:40
24-AUG-19
Client
---------Project:
Client ID:
Report Date: September 17, 2019
DNMI00107
DNMIOOI
Parameter Qualifier Result DL RL Units PF OF Analyst Date Time Batch Method -------
-lazardous Waste
\STM D 5057 Specific Gravity "As Received"
,pecific Gravity 1.02 0.010 0.100 none 1 YHl 08/30/19 1124 1913001
The following Analytical Methods were perfonned: _____________ _
\.fethod Descri tion Analyst Comments
ASTMD 5057
~otes:
)RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 18 of 50 SDG: 488668 Revl
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company:
Address:
Energy Fuels Resources (USA), Inc .
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Contact: Ms. Kathy Weinel
Project: Tailings 2019 Characterization ------Client Sample ID: Cell 4A
Sample ID: 488668004
Matrix: Water
Collect Date: 21-AUG-19 09:40
Receive Date: 24-AUG-19
Collector: Client
Parameter Qualifier Result Uncertainty
-Iigh Rad Testing
\lphaspec Th, Liquid "As Received"
:·horium-228 941
:horium-230 4.30E+05
:horium-232 2870
]FPC,Total Alpha Radium, Liquid "As Received"
}ross Radium Alpha 2.61E+05
~ucas Cell, Ra226, liquid "As Received"
tadium-226 260
J-233/234,U-235/236 and U-238 "As Received"
Jranium-233/234
Jranium-235/236
Jranium-238
9350
674
10900
[he following Prep Methods were performed:
Vlethod Description
}L-RAD-A-026 Laboratory Filtration
The following Analytical Methods were performed:
Method Descri tion
+/-274
+/-5180
+/-431
+/-2840
+/-25.2
+/-865
+/-273
+/-926
DOE EML HASL-300, Th-01-RC Modified
EPA 903.0
EPA 903.1 Modified
DOE EML HASL-300, U-02-RC Modified
;urrogate/Tracer Recovery Test
Alphaspec Th, Liquid "As Received"
MDC
534
565
387
411
31.8
626
289
432
ihorium-229 Tracer
3arium Carrier
Jranium-232 Tracer
GFPC,Total Alpha Radium, Liquid "As Received"
U-233/234,U-235/236 and U-238 "As Received"
~otes:
RL
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Analyst
:.':ounting Uncertainty is calculated at the 68% confidence level (I-sigma).
Project:
Client ID:
DNMI00107
DNMI001
Units PF DF Analyst Date Time Batch Method
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
Date
Result
JXB7 09/11/19 1927 1914167
AXM6 09/12/19 1658 1914172
MXH8 09/12/19 1034 1914039
JXB7 09/12/19 1204 1914171
Time Prep Batch
1912341
Anal st Comments
Nominal Recovery%
105
99.4
82.7
Acceptable Limits
(15%-125%)
(25%-125%)
(15%-125%)
2
3
4
;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Page 37 of 50 SDG: 488668 Revl
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company:
Address:
Contact:
Project:
Client Sample ID:
Sample ID:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 2019 Characterization
Cell 4A
488668004
Parameter Qualifier Result Uncertainty MDC
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
RL
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 38 of 50 SDG: 488668 Revl
Project:
Client ID:
DNMI00107
DNMI001
Units PF DF Analyst Date Time Batch Method
EI\ERGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.688.7175 • Helena, MT 877.472.0711
LABO RA TORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-005
Client Sample ID: Cell 4A LOS
Analyses Result Units Qualifiers
MAJOR IONS
Alkalinity, Total as CaC03 ND mg/L
Carbonate as C03 ND mg/L
Bicarbonate as HC03 ND mg/L
Chloride 7360 mg/L D
Fluoride 1530 mg/L D
Sulfate 72600 mg/L D
PHYSICAL PROPERTIES
Conductivity @ 25 C 75400 umhos/cm E
pH 2.39 s.u. H
pH Measurement Temp 17 ·c
Solids, Total Dissolved TDS@ 180 C 112000 mg/L D
NUTRIENTS
Nitrogen, Nitrate+Nitrite as N 58.2 mg/L D
Nitrogen, Ammonia as N 6080 mg/L D
METALS, DISSOLVED
Arsenic 52 mg/L
Beryllium 0.37 mg/L
Cadmium 1.9 mg/L
Calcium 520 mg/L
Chromium 6.5 mg/L
Cobalt 25 mg/L
Copper 500 mg/L
Iron 2500 mg/L
Lead 4.2 mg/L
Magnesium 3800 mg/L
Manganese 190 mg/L
Mercury 1.4 ug/L
Molybdenum 8.4 mg/L
Nickel 46 mg/L
Potassium 1000 mg/L
Selenium 3.1 mg/L
Silver 0.23 mg/L
Sodium 13000 mg/L
Thallium 0.055 mg/L
Tin ND mg/L
Uranium 38 mg/L
Vanadium 130 mg/L
Zinc 210 mg/L
VOLATILE ORGANIC COMPOUNDS
Tetrahydrofuran 16 ug/L
Report RL -Analyte reporting limit.
Definitions: QCL -Quality control limit.
D -RL increased due to sample matrix.
H -Analysis performed past recommended holding time.
MCU
RL QCL
5
5
5
100
50
400
5
0.01
1000
0.2
1000
0.4
0.02
0.02
70
4
0.07
2
0.1
20
0.1
0.2
0.2
0.2
40
0.2
0.07
40
0.07
0.07
0.04
4
0.7
35.0
Report Date: 11 /25/19
Collection Date: 08/21/19 09:45
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date I By
A2320 B 08/23/19 15:59 / dmb
A2320 B 08/23/19 15:59 / dmb
A2320 B 08/23/19 15:59 I dmb
E300.0 09/10/19 14:09 / ljl
A4500-F C 08/26/19 18:44 / dmb
E300.0 09/10/19 14:09 / ljl
A2510 B 08/23/19 11 :46 / kjp
A4500-H B 08/23/19 11 :46 / kjp
A4500-H B 08/23/19 11 :46 / kjp
A2540 C 08/26/19 16: 11 / kjp
E353.2 08/27/19 12:12 / dmb
E350.1 08/26/19 18:10 I dmb
E200.7 _8 10/26/19 06:44 I ta-a
E200.7_8 10/26/19 06:44 I ta-a
E200.7 _8 10/26/19 06:44 / ta-a
E200.7_8 10/26/19 06:44 / ta-a
E200.7 _8 10/26/19 06:44 I ta-a
E200.7 _8 10/26/19 06:44 I ta-a
E200.7 _8 10/26/19 06:44 I ta-a
E200.7_8 10/26/19 06:44 I ta-a
E200.7 _8 10/26/19 06:44 I ta-a
E200.7 _8 10/26/19 06:44 I ta-a
E200.7 _8 10/26/19 06:44 / ta-a
E245.1 09/09/19 19:52 / ta-a
E200.7_8 10/26/19 06:44 / ta-a
E200.7_8 10/26/19 06:44 / ta-a
E200.7_8 10/26/19 06:44 I ta-a
E200.7_8 10/26/19 06:44 I ta-a
E200.7_8 10/26/19 06:44 I ta-a
E200.7_8 10/26/19 06:44 / ta-a
E200.7 _8 10/26/19 06:44 I ta-a
E200.7_8 10/26/19 06:44 / ta-a
E200.7_8 10/26/19 06:44 I ta-a
E200.7_8 10/26/19 06:44 / ta-a
E200.7_8 10/26/19 06:44 I ta-a
SW8260B 09/03/19 15:53 / ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
E -Estimated value. Result exceeds the instrument upper
quantitation limit.
Page 25 of 172
EI\ERGY
'
•' Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Giflette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C19081073-005
Client Sample ID: Cell 4A LOS
Analyses Result Units Qualifiers
VOLATILE ORGANIC COMPOUNDS
Acetone 84 ug/L
Acetonitrile 116 ug/L
Acrolein ND ug/L
Acrylonitrile ND ug/L
Benzene ND ug/L
Bromobenzene ND ug/L
Bromochloromethane ND ug/L
Bromodichloromethane ND ug/L
Bromoform ND ug/L
Bromomethane ND ug/L
n-Butylbenzene ND ug/L
sec-Butylbenzene ND ug/L
tert-Butylbenzene ND ug/L
Carbon disulfide 0.72 ug/L J
Carbon tetrachloride ND ug/L
Chlorobenzene ND ug/L
Chlorodibromomethane ND ug/L
Chloroethane 5.7 ug/L
2-Chloroethyl vinyl ether ND ug/L
Chloroform 31 ug/L
Chloromethane 3.6 ug/L
2-Chlorotoluene ND ug/L
4-Chlorotoluene ND ug/L
1,2-Dibromo-3-chloropropane ND ug/L
1,2-Dibromoethane ND ug/L
Dibromomethane ND ug/L
1,2-Dichlorobenzene ND ug/L
1,3-Dichlorobenzene ND ug/L
1,4-Dichlorobenzene ND ug/L
Dichlorodifluoromethane ND ug/L
1, 1-Dichloroethane ND ug/L
1,2-Dichloroethane ND ug/L
1, 1-Dichloroethene ND ug/L
cis-1,2-Dichloroethene ND ug/L
trans-1 ,2-Dichloroethene ND ug/L
1,2-Dichloropropane ND ug/L
1,3-Dichloropropane ND ug/L
2,2-Dichloropropane ND ug/L
1, 1-Dichloropropene ND ug/L
cis-1 ,3-Dichloropropene ND ug/L
trans-1 ,3-Dichloropropene ND ug/L
Ethylbenzene ND ug/L
Hexachlorobutadiene ND ug/L
Report RL -Analyte reporting limit.
Definitions: QCL -Quality control limit.
J -Estimated value. The analyte was present but less
than the reporting limit.
MCU
RL QCL
20
20
20
20
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Report Date: 11 /25/19
Collection Date: 08/21/19 09:45
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
SW8260B 09/04/19 11 :16 / dm
SW8260B 09/04/19 11 : 16 / dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04119 11 :16 I dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04/19 11 :16 / dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04/19 11: 16 / dm
SW8260B 09/0411911 :16 I dm
SW8260B 09104/19 11 :16 I dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04/19 11 : 16 / dm
SW8260B 09/04/1911:16 I dm
SW8260B 09/04/19 11 :16 I dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/0411911 :16 / dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04119 11 :16 I dm
SW8260B 09/04/1911:16 I dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04/19 11 :16 / dm
SW8260B 09/04/1911 :16/dm
SW8260B 09/04/19 11 : 16 / dm
SW8260B 09/04/1911:16 / dm
SW8260B 09/04/19 11:16 / dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04/1911:16 / dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04/1911:16 / dm
SW8260B 09/04/19 11 : 16 / dm
SW8260B 09/04/1911 :16 I dm
SW8260B 09/04/19 11 :16 / dm
SW8260B 09104/19 11 :16 I dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04/1911 :16 / dm
SW8260B 09/04/1911:16 / dm
SW8260B 09/04/19 11 : 16 / dm
SW8260B 09/04/19 11:16 / dm
SW8260B 09/04/19 11 :16 / dm
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 26 of 172
EI\ERGY •' Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.688. 7175 • Helena, MT 877.472.0711
LABO RA TORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 09:45
Lab ID: C 19081073-005 Date Received: 08/22/19
Client Sample ID: Cell 4A LOS Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
VOLATILE ORGANIC COMPOUNDS
2-Hexanone 71 ug/L 20 SW8260B 09/04/1911:16 I dm
lodomethane ND ug/L 1.0 SW8260B 09/04/19 11 :16 / dm
lsopropylbenzene ND ug/L 1.0 SW8260B 09/04/19 11 :16 / dm
p-lsopropyltoluene ND ug/L 1.0 SW8260B 09/04/1911 :16 / dm
Methyl tert-butyl ether (MTBE) ND ug/L 1.0 SW8260B 09/04/19 11: 16 / dm
Methyl ethyl ketone 43 ug/L 20 SW8260B 09/04/1911:16 / dm
Methyl isobutyl ketone ND ug/L 20 SW8260B 09/04/19 11:16 / dm
Methylene chloride 0.47 ug/L J 1.0 SW8260B 09/04/1911 :16 / dm
Naphthalene ND ug/L 1.0 SW8260B 09/04/1911 :16 / dm
n-Propylbenzene ND ug/L 1.0 SW8260B 09/04/19 11: 16 / dm
Styrene ND ug/L 1.0 SW8260B 09/04/19 11: 16 / dm
1, 1, 1,2-Tetrachloroethane ND ug/L 1.0 SW8260B 09/04/19 11: 16 / dm
1, 1,2,2-Tetrachloroethane ND ug/L 1.0 SW8260B 09/04/1911 :16 / dm
Tetrachloroethene ND ug/L 1.0 SW8260B 09/04/19 11 :16 / dm
Toluene ND ug/L 1.0 SW8260B 09/04/19 11: 16 / dm
1,2,3-Trichlorobenzene ND ug/L 1.0 SW8260B 09/04/1911:16 / dm
1,2,4-Trichlorobenzene ND ug/L 1.0 SW8260B 09/04/1911:16 / dm
1, 1, 1-Trichloroethane ND ug/L 1.0 SW8260B 09/04/1911 :16 / dm
1, 1,2-Trichloroethane ND ug/L 1.0 SW8260B 09/04/1911 :16 / dm
Trichloroethene ND ug/L 1.0 SW8260B 09/04/1911 :16 / dm
Trichlorofluoromethane ND ug/L 1.0 SW8260B 09/04/19 11: 16 / dm
1,2,3-Trichloropropane ND ug/L 1.0 SW8260B 09/04/1911 :16 / dm
1,2,4-Trimethylbenzene ND ug/L 1.0 SW8260B 09/04/1911 :16 / dm
1,3, 5-Trimethylbenzene ND ug/L 1.0 SW8260B 09/04/1911:16 / dm
Vinyl acetate ND ug/L 1.0 SW8260B 09/04/1911:16/ dm
Vinyl chloride ND ug/L 1.0 SW8260B 09/04/19 11: 16 / dm
m+p-Xylenes ND ug/L 1.0 SW8260B 09/04/1911 :16 / dm
o-Xylene ND ug/L 1.0 SW8260B 09/04/1911 :16 / dm
Xylenes, Total ND ug/L 1.0 SW8260B 09/04/19 11:16 / dm
Surr: 1,2-Dichloroethane-d4 126 %REC 70-130 SW8260B 09/04/19 11 : 16 / dm
Surr: Dibromofluoromethane 118 %REC 70-130 SW8260B 09/04/1911 :16 / dm
Surr: p-Bromofluorobenzene 89.0 %REC 70-130 SW8260B 09/04/1911 :16 / dm
Surr: Toluene-dB 84.0 %REC 70-130 SW8260B 09/04/1911:16 / dm
SEMI-VOLATILE ORGANIC COMPOUNDS
1,2,4-Trichlorobenzene ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
1,2-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
1,3-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
1,4-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
1-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
2,4, 5-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
2,4,6-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
2,4-Dichlorophenol ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time. J -Estimated value. The analyte was present but less
than the reporting limit.
Page 27 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WV 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABO RA TORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21 /19 09:45
Lab ID: C 19081073-005 DateReceived: 08/22/19
Client Sample ID: Cell 4A LOS Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
SEMI-VOLATILE ORGANIC COMPOUNDS
2,4-Dimethylphenol ND ug/L H 10 SW8270C 09/12/19 22:19 / ta-a
2,4-Dinitrophenol ND ug/L H 50 SW8270C 09/12/19 22: 19 / ta-a
2,4-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/1922: 19 / ta-a
2,6-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
2-Chloronaphthalene ND ug/L H 10 SW8270C 09/12/1922: 19 / ta-a
2-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 22:19 / ta-a
2-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
2-Nitrophenol ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
3,3 · -Dichlorobenzidine ND ug/L H 46 SW8270C 09/12/19 22: 19 / ta-a
4,6-Dinitro-2-methylphenol ND ug/L H 50 SW8270C 09/12/1922: 19 / ta-a
4-Bromophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
4-Chloro-3-methylphenol ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
4-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
4-Chlorophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
4-Nitrophenol ND ug/L H 50 SW8270C 09/12/19 22: 19 / ta-a
Acenaphthene ND ug/L H 10 SW8270C 09/12/19 22:19 / ta-a
Acenaphthylene ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
Anthracene ND ug/L H 10 SW8270C 09112119 22: 19 I ta-a
Azobenzene ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
Benzidine ND ug/L H 10 SW8270C 09/12/19 22:19 / ta-a
Benzo(a)anthracene ND ug/L H 10 SW8270C 09/12/19 22:19 / ta-a
Benzo(a)pyrene ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
Benzo(b)fluoranthene ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
Benzo(g, h, i)perylene ND ug/L H 10 SW8270C 09/12119 22: 19 / ta-a
Benzo(k)fluoranthene ND ug/L H 10 SW8270C 09/12/1922: 19 / ta-a
bis(-2-chloroethoxy)Methane ND ug/L H 10 SW8270C 09112/19 22: 19 / ta-a
bis(-2-ch loroethyl)Ether ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
bis(2-chloroisopropyl)Ether ND ug/L H 10 SW8270C 09/12/19 22:19 / ta-a
bis(2-ethylhexyl)Phthalate 1.1 ug/L H 10 SW8270C 09112/19 22: 19 / ta-a
Butylbenzylphthalate ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
Chrysene ND ug/L H 10 SW8270C 09/12/19 22:19 / ta-a
Di-n-butyl phthalate ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
Di-n-octyl phthalate ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
Dibenzo(a,h)anthracene ND ug/L H 10 SW8270C 09112/19 22:19 I ta-a
Diethyl phthalate ND ug/L H 10 SW8270C 09/12119 22: 19 I ta-a
Dimethyl phthalate ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
Fluoranthene ND ug/L H 10 SW8270C 09112119 22:19 I ta-a
Fluorene ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
Hexachlorobenzene ND ug/L H 10 SW8270C 09/12/19 22:19 / ta-a
Hexachlorobutadiene ND ug/L H 28 SW8270C 09/12/19 22: 19 / ta-a
Hexachlorocyclopentadiene ND ug/L H 10 SW8270C 09/12/19 22: 19 / ta-a
Hexachloroethane ND ug/L H 28 SW8270C 09/12/19 22:19 I ta-a
lndeno(1,2,3-cd)pyrene ND ug/L H 10 SW8270C 09/12119 22: 19 I ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time.
Page 28 of 172
EI\ERGY
' '
Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-005
Client Sample ID: Cell 4A LOS
Analyses
SEMI-VOLATILE ORGANIC COMPOUNDS
lsophorone
m+p-Cresols
n-Nitroso-di-n-propylamine
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
o-Cresol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Qualifiers
H
H
H
H
H
H
H
H
H
H
H
H
H
H -Analysis performed past recommended holding time.
MCU
RL QCL
10
10
10
10
10
10
10
10
50
10
10
10
19
Report Date: 11/25/19
Collection Date: 08/21/19 09:45
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
SW8270C 09/12/19 22: 19 / ta-a
SW8270C 09/12/19 22: 19 / ta-a
SW8270C 09/12/19 22: 19 / ta-a
SW8270C 09/12/19 22: 19 / ta-a
SW8270C 09/12/19 22:19 / ta-a
SW8270C 09/12/19 22: 19 / ta-a
SW8270C 09/12/19 22: 19 / ta-a
SW8270C 09/12/19 22: 19 / ta-a
SW8270C 09/12/19 22: 19 / ta-a
SW8270C 09/12/19 22: 19 / ta-a
SW8270C 09/12/19 22: 19 / ta-a
SW8270C 09/12/19 22: 19 / ta-a
SW8270C 09/12/19 22:19 / ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 29 of 172
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Company:
Address:
Certificate of Analysis
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Contact: Ms. Kathy Weinel
Project: Tailings 2019 Characterization
Report Date: September 17, 2019
-----------------------------------Client Sample ID: Cell 4A LDS
Sample ID: 488668005
Matrix: Water
Collect Date: 21-AUG-19 09:45
Receive Date: 24-AUG-19
Collector: Client
Project:
Client ID:
DNMI00107
DNMIOOI
-------
Parameter
-lazardous Waste
Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method ------------------------~
\STM D 5057 Specific Gravity "As Received"
;pecific Gravity 1.02 0.010 0.100 none I VHI 08/30/19 1124 1913001
The following Analytical Methods were perfonned: -----'---------------------------------\1ethod Descri tion Analyst Comments
ASTMD 5057
'fotes:
)RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Column headers are defined as follows:
OF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 19 of 50 SDG: 488668 Revl
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company:
Address:
Contact:
Project:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 2019 Characterization --------------Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Ce 114 A LDS
488668005
Water
21-AUG-19 09:45
24-AUG-19
Client
Parameter Qualifier Result Uncertainty
-Iigh Rad Testing
\lphaspec Th, Liquid "As Received"
'horium-228 1060 +/-279
'horium-230 3.66E+05 +/-4840
'.horium-232 2230 +/-383
]FPC,Total Alpha Radium, Liquid "As Received"
}ross Radium Alpha 1.63E+05 +/-1990
Jucas Cell, Ra226, liquid "As Received"
tadium-226 73.4 +/-13.2
J-233/234,U-235/236 and U-238 "As Received"
Jranium-233/234 13500 +/-985
Jranium-235/236 738 +/-276
Jranium-238 13000 +/-965
fhe following Prep Methods were perfonned:
viethod Description
}L-RAD-A-026 Laboratory Filtration
The following Analytical Methods were performed:
\1.ethod Descri tion
DOE EML HASL-300, Th-01-RC Modified
EPA 903.0
EPA 903.1 Modified
DOE EML HASL-300, U-02-RC Modified
:;urrogate/Tracer Recovery Test
Alphaspec Th, Liquid "As Received"
MDC
402
524
246
275
22.5
631
480
587
fhorium-229 Tracer
3arium Carrier
Jranium-232 Tracer
GFPC,Total Alpha Radium, Liquid "As Received"
U-233/234,U-235/236 and U-238 "As Received"
~otes:
RL
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Analyst
:::ounting Uncertainty is calculated at the 68% confidence level (I-sigma).
Project:
Client ID:
DNMI00107
DNMIOOI
Units PF DF Analyst Date Time Batch Method
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
Date
Result
JXB7 09/11/19 1927 1914167
AXM6 09/12/19 1658 1914172 2
MXH8 09/16/19 1124 1914039 3
JXB7 09/11/19 1927 1914171 4
Time Prep Batch
1912341
Anal st Comments
Nominal Recovery%
86
101
88.1
Acceptable Limits
(15%-125%)
(25%-125%)
(15%-125%)
,RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Page 39 of 50 SDG: 488668 Revl
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Company :
Address:
Contact:
Project:
Client Sample ID:
Sample ID:
-------
Certificate of Analysis
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 2019 Characterization ------------Ce 114 A LDS
488668005
Project:
Client ID:
Report Date: September 17, 2019
DNMI00107
DNMIOOI
Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 40 of 50 SDG: 488668 Revl
--------
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
EN:RGY
' '
.-Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-006
Client Sample ID: Cell 48
Analyses Result Units Qualifiers
MAJOR IONS
Alkalinity, Total as CaC03 ND mg/L
Carbonate as C03 ND mg/L
Bicarbonate as HC03 ND mg/L
Chloride 10500 mg/L D
Fluoride 2300 mg/L D
Sulfate 124000 mg/L D
PHYSICAL PROPERTIES
Conductivity @ 25 C 99600 umhos/cm E
pH 1.53 s.u. H
pH Measurement Temp 17 oc
Solids, Total Dissolved TDS @ 180 C 180000 mg/L D
NUTRIENTS
Nitrogen, Nitrate+Nitrite as N 38.6 mg/L D
Nitrogen, Ammonia as N 8150 mg/L D
METALS, DISSOLVED
Arsenic 140 mg/L
Beryllium 0.64 mg/L
Cadmium 2.0 mg/L
Calcium 670 mg/L
Chromium 12 mg/L
Cobalt 44 mg/L
Copper 830 mg/L
Iron 5800 mg/L
Lead 16 mg/L
Magnesium 6500 mg/L
Manganese 320 mg/L
Mercury 0.46 ug/L
Molybdenum 29 mg/L
Nickel 78 mg/L
Potassium 1900 mg/L
Selenium 6.6 mg/L
Silver 0.17 mg/L
Sodium 18000 mg/L
Thallium ND mg/L
Tin 0.34 mg/L
Uranium 36 mg/L
Vanadium 710 mg/L
Zinc 280 mg/L
VOLATILE ORGANIC COMPOUNDS
Tetrahydrofuran ND ug/L
Report RL -Analyte reporting limit.
Definitions: QCL -Quality control limit.
D -RL increased due to sample matrix.
H -Analysis performed past recommended holding time.
MCU
RL QCL
5
5
5
100
50
400
5
0.01
1000
0.2
1000
0.5
0.02
0.02
100
5
0.1
2
2
0.2
20
0.2
0.2
0.2
0.2
50
0.2
0.1
50
0.1
0.1
0.05
5
35.0
Report Date: 11 /25/19
Collection Date: 08/21/19 10:15
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
A2320 B 08/23/19 16:05 I dmb
A2320 B 08/23/19 16:05 I dmb
A2320 B 08/23/19 16:05 / dmb
E300.0 09/10/19 14:28 / ljl
A4500-F C 08/26/19 18:51 / dmb
E300.0 09/10/19 14:28 / ljl
A2510 B 08/23/19 11 :49 I kjp
A4500-H B 08/23/19 11 :49 / kjp
A4500-H B 08/23/19 11 :49 I kjp
A2540 C 08/23/19 14:04 I kjp
E353.2 08/27/19 12:13 / dmb
E350.1 08/26/19 18: 14 / dmb
E200.7_8 10/26/19 06:51 / ta-a
E200.7_8 10/26/19 06:51 I ta-a
E200.7_8 10/26/19 06:51 /ta-a
E200.7_8 10/26/19 06:51 I ta-a
E200.7_8 10/26/19 06:51 / ta-a
E200.7_8 10/26/19 06:51 I ta-a
E200.7 _8 10/26/19 06:51 I ta-a
E200.7 _8 10/26/19 06:51 / ta-a
E200.7 _8 10/26/19 06:51 I ta-a
E200.7 _8 10/26/19 06:51 I ta-a
E200.7 _8 10/26/19 06:51 I ta-a
E245.1 09/09/19 19:54 I ta-a
E200.7 _8 10/26/19 06:51 / ta-a
E200.7 _8 10/26/19 06:51 / ta-a
E200.7_8 10/26/19 06:51 / ta-a
E200.7_8 10/26/19 06:51 I ta-a
E200.7 _8 10/26/19 06:51 I ta-a
E200.7 _8 10/26/19 06:51 / ta-a
E200.7 _8 10/26/19 06:51 / ta-a
E200.7 _8 10/26/19 06:51 I ta-a
E200.7 _8 10/26/19 06:51 / ta-a
E200.7 _8 10/26/19 06:51 I ta-a
E200.7 _8 10/26/19 06:51 I ta-a
SW8260B 09/03/19 16:14 / ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
E -Estimated value. Result exceeds the instrument upper
quantitation limit.
Page 30 of 172
EN:RGY ~· Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C19081073-006
Client Sample ID: Cell 4B
Analyses Result Units Qualifiers
VOLATILE ORGANIC COMPOUNDS
Acetone 39 ug/L
Acetonitrile 66 ug/L
Acrolein ND ug/L
Acrylonitrile ND ug/L
Benzene ND ug/L
Bromobenzene ND ug/L
Bromochloromethane ND ug/L
Bromodichloromethane ND ug/L
Bromoform ND ug/L
Bromomethane ND ug/L
n-Butylbenzene ND ug/L
sec-Butyl benzene ND ug/L
tert-Butylbenzene ND ug/L
Carbon disulfide ND ug/L
Carbon tetrachloride ND ug/L
Chlorobenzene ND ug/L
Chlorodibromomethane ND ug/L
Chloroethane 2.7 ug/L
2-Chloroethyl vinyl ether ND ug/L
Chloroform 3.4 ug/L
Chloromethane 2. 1 ug/L
2-Chlorotoluene ND ug/L
4-Chlorotoluene ND ug/L
1,2-Dibromo-3-chloropropane ND ug/L
1,2-Dibromoethane ND ug/L
Dibromomethane ND ug/L
1,2-Dichlorobenzene ND ug/L
1,3-Dichlorobenzene ND ug/L
1,4-Dichlorobenzene ND ug/L
Dichlorodifluoromethane ND ug/L
1, 1-Dichloroethane ND ug/L
1,2-Dichloroethane ND ug/L
1, 1-Dichloroethene ND ug/L
cis-1,2-Dichloroethene ND ug/L
trans-1,2-Dichloroethene ND ug/L
1,2-Dichloropropane ND ug/L
1,3-Dichloropropane ND ug/L
2,2-Dichloropropane ND ug/L
1, 1-Dichloropropene ND ug/L
cis-1,3-Dichloropropene ND ug/L
trans-1,3-Dichloropropene ND ug/L
Ethylbenzene ND ug/L
Hexachlorobutadiene ND ug/L
Report RL -Analyte reporting limit.
Definitions: QCL -Quality control limit.
J -Estimated value. The analyte was present but less
than the reporting limit.
MCU
RL QCL
20
20
20
20
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Report Date: 11/25/19
Collection Date: 08/21/19 10:15
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date I By
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04119 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04119 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04119 09:41 / dm
SW8260B 09/04119 09:41 / dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04119 09:41 / dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04119 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 / dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04/19 09:41 I dm
SW8260B 09/04119 09:41 I dm
SW8260B 09/04/19 09:41 I dm
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 31 of 172
EI\ERGY • Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LA BORA TORY ANAL YT I CAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 10:15
Lab ID: C 19081073-006 DateReceived: 08/22/19
Client Sample ID: Cell4B Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date I By
VOLATILE ORGANIC COMPOUNDS
2-Hexanone 5.3 ug/L J 20 SW8260B 09/04/19 09:41 / dm
lodomethane ND ug/L 1.0 SW8260B 09/04/19 09:41 / dm
lsopropylbenzene ND ug/L 1.0 SW8260B 09/04/19 09:41 / dm
p-lsopropyltoluene ND ug/L 1.0 SW8260B 09/04/19 09:41 / dm
Methyl tert-butyl ether (MTBE) ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
Methyl ethyl ketone 15 ug/L J 20 SW8260B 09/04/19 09:41 I dm
Methyl isobutyl ketone ND ug/L 20 SW8260B 09/04/19 09:41 I dm
Methylene chloride ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
Naphthalene ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
n-Propylbenzene ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
Styrene ND ug/L 1.0 SW8260B 09/04/19 09:41 / dm
1, 1, 1,2-Tetrachloroethane ND ug/L 1.0 SW8260B 09/04/19 09:41 / dm
1, 1,2,2-Tetrachloroethane ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
Tetrachloroethene ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
Toluene ND ug/L 1.0 SW8260B 09/04/19 09:41 / dm
1,2,3-Trichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
1,2,4-Trichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 09:41 / dm
1, 1, 1-Trichloroethane ND ug/L 1.0 SW8260B 09/04/19 09:41 / dm
1, 1,2-Trichloroethane ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
Trichloroethene ND ug/L 1.0 SW8260B 09/04/19 09:41 / dm
Trichlorofluoromethane ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
1,2,3-Trichloropropane ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
1,2,4-Trimethylbenzene ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
1,3,5-Trimethylbenzene ND ug/L 1.0 SW8260B 09/04/19 09:41 / dm
Vinyl acetate ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
Vinyl chloride ND ug/L 1.0 SW8260B 09/04/19 09:41 / dm
m+p-Xylenes ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
o-Xylene ND ug/L 1.0 SW8260B 09/04/19 09:41 I dm
Xylenes, Total ND ug/L 1.0 SW8260B 09/04/19 09:41 / dm
Surr: 1,2-Dichloroethane-d4 123 %REC 70-130 SW8260B 09/04/19 09:41 / dm
Surr: Dibromofluoromethane 118 %REC 70-130 SW8260B 09/04/19 09:41 / dm
Surr: p-Bromofluorobenzene 100 %REC 70-130 SW8260B 09/04/19 09:41 / dm
Surr: Toluene-dB 80.0 %REC 70-130 SW8260B 09/04/19 09:41 I dm
SEMI-VOLATILE ORGANIC COMPOUNDS
1,2,4-Trichlorobenzene ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
1,2-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
1,3-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
1,4-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
1-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
2,4,5-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
2,4,6-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
2,4-Dichlorophenol ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time. J -Estimated value. The analyte was present but less
than the reporting limit.
Page 32 of 172
EI\ERGY
' ' '
•' Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 10:15
Lab ID: C 19081073-006 DateReceived: 08/22/19
Client Sample ID: Cell4B Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
SEMI-VOLATILE ORGANIC COMPOUNDS
2,4-Dimethylphenol ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
2,4-Dinitrophenol ND ug/L H 50 SW8270C 09/12/19 22:49 I ta-a
2,4-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
2,6-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
2-Chloronaphthalene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
2-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
2-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
2-Nitrophenol ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
3,3 · -Dichlorobenzidine ND ug/L H 44 SW8270C 09/12/19 22:49 / ta-a
4,6-Dinitro-2-methylphenol ND ug/L H 50 SW8270C 09/12/19 22:49 / ta-a
4-Bromophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
4-Chloro-3-methylphenol ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
4-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
4-Chlorophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
4-Nitrophenol ND ug/L H 50 SW8270C 09/12/19 22:49 I ta-a
Acenaphthene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Acenaphthylene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Anthracene 1.7 ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Azobenzene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Benzidine ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
Benzo(a)anthracene ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
Benzo(a)pyrene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Benzo(b)fluoranthene ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
Benzo(g, h, i)perylene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Benzo(k)fluoranthene ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
bis(-2-chloroethoxy)Methane ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
bis(-2-chloroethyl)Ether ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
bis(2-chloroisopropyl)Ether ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
bis(2-ethylhexyl)Phthalate ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Butylbenzylphthalate ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
Chrysene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Di-n-butyl phthalate ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Di-n-octyl phthalate ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Dibenzo(a,h)anthracene ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
Diethyl phthalate ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
Dimethyl phthalate ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Fluoranthene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Fluorene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Hexachlorobenzene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Hexachlorobutadiene ND ug/L H 26 SW8270C 09/12/19 22:49 I ta-a
Hexachlorocyclopentadiene ND ug/L H 10 SW8270C 09/12/19 22:49 I ta-a
Hexachloroethane ND ug/L H 26 SW8270C 09/12/19 22:49 / ta-a
lndeno(1,2,3-cd)pyrene ND ug/L H 10 SW8270C 09/12/19 22:49 / ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time.
Page 33 of 172
EI\ERGY Trust our People. Trust our Data.
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Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686. 7175 • Helena, MT 877.472.0711
LABO RA TORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-006
Client Sample ID: Cell 48
Analyses
SEMI-VOLATILE ORGANIC COMPOUNDS
lsophorone
m+p-Cresols
n-Nitroso-di-n-propylamine
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
o-Cresol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Qualifiers
H
H
H
H
H
H
H
H
H
H
H
H
H
H -Analysis performed past recommended holding time.
MCU
RL QCL
10
10
10
10
10
10
10
10
50
10
10
10
18
Report Date: 11 /25/19
Collection Date: 08/21/1910:15
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date I By
SW8270C 09/12/19 22:49 I ta-a
SW8270C 09/12/19 22:49 I ta-a
SW8270C 09/12/19 22:49 I ta-a
SW8270C 09/12/19 22:49 I ta-a
SW8270C 09/12/19 22:49 I ta-a
SW8270C 09/12/19 22:49 I ta-a
SW8270C 09/12/19 22:49 I ta-a
SW8270C 09/12/19 22:49 / ta-a
SW8270C 09/12/19 22:49 / ta-a
SW8270C 09/12/19 22:49 I ta-a
SW8270C 09/12/19 22:49 I ta-a
SW8270C 09/12/19 22:49 / ta-a
SW8270C 09/12/19 22:49 / ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 34 of 172
Company :
Address:
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 2019 Characterization
Cell 4B
488668006
Water
21-AUG-19 10:15
24-AUG-19
Client
Project:
Client ID:
Report Date: September 17, 2019
DNMI00107
DNMI001
Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method
-Iazardous Waste
'\.STM D 5057 Specific Gravity "As Received"
,pecific Gravity ' 1.10 0.010 0.100 none I VHI 08/30/19 1124 1913001
The following Analytical Methods were perfonned: ----=--------------------\1 et hod Descri tion Anal st Commen~t~s _________ _
ASTMD 5057
~otes:
:;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC : Minimum Detectable Concentration
Page 20 of 50 SDG: 488668 Revl
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company:
Address:
Contact:
Project:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 2019 Characterization -----------
Parameter
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Ce 114 B
488668006
Water
21-AUG-19 10:15
24-AUG-19
Client
Qualifier Result Uncertainty MDC RL
Project:
Client ID:
DNMI00107
DNMIOOI
Units PF OF Analyst Date Time Batch Method ------------Iigh Rad Testing
\lphaspec Th, Liquid "As Received"
~horium-228 1080 +/-262 411 1.00 pCi/L JXB7 09/11/19 1927 1914167
~horium-230 4.34E+05 +/-4850 437 1.00 pCi/L
"horium-232 3490 +/-440 308 1.00 pCi/L
}FPC,Total Alpha Radium, Liquid "As Received"
}ross Radium Alpha 3.10E+05 +/-3100 307 1.00 pCi/L AXM6 09/12/19 1658 1914172 2
Jucas Cell, Ra226, liquid "As Received"
tadium-226 296 +/-27.1 30.8 1.00 pCi/L MXH8 09/12/19 1034 1914039 3
J-233/234,U-235/236 and U-238 "As Received"
Jranium-233/234 11600 +/-864 586 1.00 pCi/L JXB7 09/11/19 1927 1914171 4
Jranium-235/236 563 +/-235 472 1.00 pCi/L
Jranium-238 10800 +/-829 505 1.00 pCi/L
rhe following Prep Methods were performed:
vfethod Date Description Analyst
}L-RAD-A-026 Laboratory Filtration
Time Prep Batch =-=----cc=--c-=-,--------=--=------------------=------------------
The following Analytical Methods were performed:
Method Descri tion
DOE EML HASL-300, Th-01-RC Modified
EPA 903.0
EPA 903.1 Modified
DOE EML HASL-300, U-02-RC Modified
;urrogate/Tracer Recovery
rhorium-229 Tracer
Test
Alphaspec Th, Liquid "As Received"
3arium Carrier
Jranium-232 Tracer
~otes:
GFPC,Total Alpha Radium, Liquid "As Received"
U-233/234,U-235/236 and U-238 "As Received"
:ounting Uncertainty is calculated at the 68% confidence level (I-sigma).
Result
19I234 l
Analvst Comm=-'-'en=t=s-~---------
Nominal Recovery%
97.9
101
93.9
Acceptable Limits
(15%-125%)
(25%-125%)
(15%-125%)
;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Page 41 of 50 SDG: 488668 Revl
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company :
Address:
Contact:
Project:
Client Sample ID:
Sample ID:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 2019 Characterization
Cell 4B
488668006
Parameter Qualifier Result Uncertainty MDC
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
RL
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 42 of 50 SDG: 488668 Revl
Project:
Client ID:
DNMI00107
DNMIOOl
Units PF DF Analyst Date Time Batch Method
EI\ERGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C19081073-007
Client Sample ID: Cell 48 LOS
Analyses Result Units Qualifiers
MAJOR IONS
Alkalinity, Total as CaC03 ND mg/L
Carbonate as C03 ND mg/L
Bicarbonate as HC03 ND mg/L
Chloride 8050 mg/L D
Fluoride 1680 mg/L D
Sulfate 89500 mg/L D
PHYSICAL PROPERTIES
Conductivity @ 25 C 80800 umhos/cm E
pH 1.73 s.u. H
pH Measurement Temp 17 ·c
Solids, Total Dissolved TDS @ 180 C 131000 mg/L D
NUTRIENTS
Nitrogen, Nitrate+Nitrite as N 41 .2 mg/L D
Nitrogen, Ammonia as N 7080 mg/L D
METALS, DISSOLVED
Arsenic 89 mg/L
Beryllium 0.47 mg/L
Cadmium 2.0 mg/L
Calcium 550 mg/L
Chromium 9.1 mg/L
Cobalt 31 mg/L
Copper 550 mg/L
Iron 4400 mg/L
Lead 7.8 mg/L
Magnesium 4800 mg/L
Manganese 240 mg/L
Mercury 0.11 ug/L
Molybdenum 27 mg/L
Nickel 59 mg/L
Potassium 1400 mg/L
Selenium 4.7 mg/L
Silver 0.17 mg/L
Sodium 13000 mg/L
Thallium 0.087 mg/L
Tin 0.20 mg/L
Uranium 31 mg/L
Vanadium 760 mg/L
Zinc 280 mg/L
VOLATILE ORGANIC COMPOUNDS
Tetrahydrofuran 53 ug/L
Report RL -Analyte reporting limit.
Definitions: QCL -Quality control limit.
D -RL increased due to sample matrix.
H -Analysis performed past recommended holding time.
MCU
RL QCL
5
5
5
100
50
400
5
0.01
1000
0.2
1000
0.5
0.02
0.02
100
5
0.1
2
2
0.2
20
0.2
0.2
0.2
0.2
50
0.2
0.1
50
0.1
0.1
0.05
5
35.0
Report Date: 11 /25/19
Collection Date: 08/21/19 10:30
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
A2320 B 08/23/19 16:08 / dmb
A2320 B 08/23/19 16:08 / dmb
A2320 B 08/23/19 16:08 / dmb
E300.0 09110/19 14:47 / ljl
A4500-F C 08/26/19 18:55 / dmb
E300.0 09/10/19 14:4 7 / ljl
A2510 B 08/23/19 11 :52 / kjp
A4500-H B 08/23/19 11 :52 / kjp
A4500-H B 08/23/19 11 :52 / kjp
A2540 C 08/23/19 14:04 / kjp
E353.2 08/27/19 12:15 / dmb
E350.1 08/26/19 18: 15 / dmb
E200.7_8 10/26/19 06:58 / ta-a
E200.7_8 10/26/19 06:58 / ta-a
E200.7_8 10/26/19 06:58 / ta-a
E200.7_8 10/26/19 06:58 / ta-a
E200.7_8 10/26/19 06:58 / ta-a
E200.7_8 10/26119 06:58 I ta-a
E200.7 _8 10/26/19 06:58 / ta-a
E200.7 _8 10/26/19 06:58 / ta-a
E200.7_8 10/26119 06:58 / ta-a
E200.7_8 10/26/19 06:58 / ta-a
E200.7_8 10/26/19 06:58 / ta-a
E245.1 09/09119 20:01 / ta-a
E200.7_8 10/26/19 06:58 I ta-a
E200.7 _8 10/26/19 06:58 I ta-a
E200.7 _8 10/26119 06:58 / ta-a
E200.7_8 10/26/19 06:58 / ta-a
E200.7_8 10126119 06:58 / ta-a
E200.7 _8 10/26/19 06:58 / ta-a
E200.7_8 10/26/19 06:58 / ta-a
E200.7_8 10/26/19 06:58 / ta-a
E200.7_8 10/26/19 06:58 / ta-a
E200.7_8 10/26/19 06:58 / ta-a
E200.7 _8 10/26119 06:58 / ta-a
SW8260B 09/03/19 16:35 / ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
E -Estimated value. Result exceeds the instrument upper
quantitation limit.
Page 35 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686. 7175 • Helena, MT 877 .472.0711
LAB ORA TORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 10:30
Lab ID: C 19081073-007 Date Received: 08/22/19
Client Sample ID: Cell 48 LOS Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
VOLATILE ORGANIC COMPOUNDS
Acetone 102 ug/L 20 SW8260B 09/04/19 10:12 / dm
Acetonitrile ND ug/L 20 SW8260B 09/04/19 10:12 / dm
Acrolein ND ug/L 20 SW8260B 09/04/19 10: 12 / dm
Acrylonitrile ND ug/L 20 SW8260B 09/04/19 10:12 / dm
Benzene ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
Bromobenzene ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
Bromochloromethane ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
Bromodichloromethane ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
Bromoform ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
Bromomethane ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
n-Butylbenzene ND ug/L 1.0 SW82608 09/04/1910:12/dm
sec-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
tert-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
Carbon disulfide ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
Carbon tetrachloride ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
Chlorobenzene ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
Chlorodibromomethane ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
Chloroethane 2.5 ug/L 1.0 SW82608 09/04/19 10:12 / dm
2-Chloroethyl vinyl ether ND ug/L 1.0 SW82608 09/04/1910:12/dm
Chloroform 3.9 ug/L 1.0 SW8260B 09/04/19 10:12 / dm
Chloromethane 2.3 ug/L 1.0 SW82608 09/04/19 10:12 / dm
2-Chlorotoluene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
4-Chlorotoluene ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
1,2-Dibromo-3-chloropropane ND ug/L 2.0 SW8260B 09/04/1910:12/dm
1,2-Dibromoethane ND ug/L 1.0 SW8260B 09/04/1910:12/dm
Dibromomethane ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
1,2-Dichlorobenzene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
1,3-Dichlorobenzene ND ug/L 1.0 SW82608 09/04/1910:12/dm
1,4-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
Dichlorodifluoromethane ND ug/L 1.0 SW8260B 09/04/1910:12/dm
1, 1-Dichloroethane ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
1,2-Dichloroethane ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
1, 1-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
cis-1,2-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 10: 12 / dm
trans-1 ,2-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
1,2-Dichloropropane ND ug/L 1.0 SW8260B 09/04/1910:12/dm
1,3-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
2,2-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
1, 1-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
cis-1,3-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 10:12 / dm
trans-1 ,3-Dichloropropene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
Ethylbenzene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
Hexachlorobutadiene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
J -Estimated value. The analyte was present but less
than the reporting limit.
Page 36 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 10:30
Lab ID: C 19081073-007 Date Received: 08/22/19
Client Sample ID: Cell 48 LDS Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
VOLATILE ORGANIC COMPOUNDS
2-Hexanone 4.8 ug/L J 20 SW82608 09/04/19 10:12 / dm
lodomethane ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
lsopropylbenzene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
p-lsopropyltoluene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
Methyl tert-butyl ether (MTBE) ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
Methyl ethyl ketone 71 ug/L 20 SW82608 09/04/19 10:12 I dm
Methyl isobutyl ketone ND ug/L 20 SW82608 09/04/19 10:12 / dm
Methylene chloride ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
Naphthalene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
n-Propylbenzene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
Styrene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
1, 1, 1,2-Tetrachloroethane ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
1, 1,2,2-Tetrachloroethane ND ug/L 1.0 SW82608 09/04/1910:12/dm
Tetrachloroethene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
Toluene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
1,2,3-Trichlorobenzene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
1,2,4-Trichlorobenzene ND ug/L 1.0 SW82608 09/04/1910:12/dm
1, 1, 1-Trichloroethane ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
1, 1,2-Trichloroethane ND ug/L 1.0 SW82608 09/04/1910:12/dm
Trichloroethene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
Trichlorofluoromethane ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
1,2, 3-Trichloropropane ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
1,2,4-Trimethylbenzene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
1,3,5-Trimethylbenzene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
Vinyl acetate ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
Vinyl chloride ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
m+p-Xylenes ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
o-Xylene ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
Xylenes, Total ND ug/L 1.0 SW82608 09/04/19 10:12 / dm
Surr: 1,2-Dichloroethane-d4 127 %REC 70-130 SW82608 09/04/19 10:12 / dm
Surr: Dibromofluoromethane 117 %REC 70-130 SW82608 09/04/19 10:12 / dm
Surr: p-Bromofluorobenzene 97.0 %REC 70-130 SW82608 09/04/19 10:12 / dm
Surr: Toluene-dB 86.0 %REC 70-130 SW82608 09/04/1910:12/dm
SEMI-VOLATILE ORGANIC COMPOUNDS
1,2,4-Trichlorobenzene ND ug/L H 10 SW8270C 09/12/19 12:28 I ta-a
1,2-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
1,3-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 12:28 I ta-a
1,4-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 12:28 I ta-a
1-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
2,4,5-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 12:28 I ta-a
2,4,6-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
2,4-Dichlorophenol ND ug/L H 10 SW8270C 09/12/19 12:28 I ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time. J -Estimated value. The analyte was present but less
than the reporting limit.
Page 37 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686. 7175 • Helena, MT 877 .472.0711
LABO RA TORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/1910:30
Lab ID: C 19081073-007 DateReceived: 08/22/19
Client Sample ID: Cell 48 LOS Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
SEMI-VOLATILE ORGANIC COMPOUNDS
2,4-Dimethylphenol ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
2,4-Dinitrophenol ND ug/L H 50 SW8270C 09/12/19 12:28 / ta-a
2,4-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
2,6-Dinitrotoluene ND ug/L H 10 SWB270C 09/12/19 12:28 / ta-a
2-Chloronaphthalene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
2-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
2-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
2-Nitrophenol ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
3,3 · -Dichlorobenzidine ND ug/L H 45 SW8270C 09/12/19 12:28 / ta-a
4,6-Dinitro-2-methylphenol ND ug/L H 50 SW8270C 09/12/19 12:28 / ta-a
4-Bromophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
4-Chloro-3-methylphenol ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
4-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
4-Chlorophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
4-Nitrophenol ND ug/L H 50 SW8270C 09/12/19 12:28 / ta-a
Acenaphthene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Acenaphthylene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Anthracene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Azobenzene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Benzidine ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Benzo(a)anthracene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Benzo(a)pyrene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Benzo(b)fluoranthene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Benzo(g,h,i)perylene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Benzo(k)fluoranthene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
bis(-2-chloroethoxy)Methane ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
bis(-2-ch loroethyl)Ether ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
bis(2-chloroisopropyl)Ether ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
bis(2-ethylhexyl)Phthalate 16 ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Butylbenzylphthalate ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Chrysene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Di-n-butyl phthalate ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Di-n-octyl phthalate ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Dibenzo(a,h)anthracene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Diethyl phthalate ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Dimethyl phthalate ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Fluoranthene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Fluorene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Hexachlorobenzene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Hexachlorobutadiene ND ug/L H 27 SW8270C 09/12/19 12:28 / ta-a
Hexachlorocyclopentadiene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Hexachloroethane ND ug/L H 27 SW8270C 09/12/19 12:28 / ta-a
lndeno(1,2,3-cd)pyrene ND ug/L H 10 SW8270C 09/12/19 12:28 / ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time.
Page 38 of 172
EI\ERGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C19081073-007
Client Sample ID: Cell 48 LOS
Analyses
SEMI-VOLATILE ORGANIC COMPOUNDS
lsophorone
m+p-Cresols
n-Nitroso-di-n-propylamine
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
o-Cresol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND ug/L
0.42 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Qualifiers
H
H
H
H
H
H
H
H
H
H
H
H
H
H -Analysis performed past recommended holding time.
MCU
RL QCL
10
10
10
10
10
10
10
10
50
10
10
10
18
Report Date: 11/25/19
Collection Date: 08/21/19 10:30
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
SW8270C 09/12/19 12:28 / ta-a
SW8270C 09/12/19 12:28 I ta-a
SW8270C 09/12/19 12:28 I ta-a
SW8270C 09/12/19 12:28 / ta-a
SW8270C 09/12/19 12:28 / ta-a
SW8270C 09/12/19 12:28 / ta-a
SW8270C 09/12/19 12:28 / ta-a
SW8270C 09/12/19 12:28 / ta-a
SW8270C 09/12/19 12:28 / ta-a
SW8270C 09/12/19 12:28 / ta-a
SW8270C 09/12/19 12:28 I ta-a
SW8270C 09/12/19 12:28 / ta-a
SW8270C 09/12/19 12:28 I ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 39 of 172
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company:
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 2019 Characterization -----Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Cell4B LDS
488668007
Water
21-AUG-19 10:30
24-AUG-19
Client
Qualifier Result
-Iazardous Waste
\STM D 5057 Specific Gravity "As Received"
,pecific Gravity 1.05
DL
0.010
RL
0.100
Project:
Client ID:
DNMI00107
DNMI001
Units PF DF Analyst Date Time Batch Method
none I VHI 08/30/19 1124 1913001
The following Analytical Methods w_e_re_p_e_rfi_o_rm_e_d: ______________ ----------------
\1ethod Descri tion Anal st Comments
ASTMD 5057
lfotes:
;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 21 of 50 SDG: 488668 Revl
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company:
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Contact:
Lakewood, Colorado 80228
Ms. Kathy W einel
Project: Tailings 2019 Characterization
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Cell 4B LDS
488668007
Water
21-AUG-19 10:30
24-AUG-19
Client
Parameter Qualifier Result Uncertainty
-Iigh Rad Testing
\lphaspec Th, Liquid "As Received"
'horium-228 I 030
~horium-230 3.68E+05
~horium-232 2650
]FPC,Total Alpha Radium, Liquid "As Received"
}ross Radium Alpha 2.26E+05
~ucas Cell, Ra226, liquid "As Received"
tadium-226 105
J-233/234,U-235/236 and U-238 "As Received"
Jranium-233/234 8840
Jranium-235/236
Jranium-238
412
9600
fhe following Pre Methods were performed:
\1ethod Description
}L-RAD-A-026 Laboratory Filtration
The following Analytical Methods were performed:
\1ethod Description
+/-290
+/-5100
+/-440
+/-2230
+/-15.4
+/-722
+/-191
+/-749
DOE EML HASL-300, Th-01-RC Modified
EPA 903.0
EPA 903.1 Modified
DOE EML HASL-300, U-02-RC Modified
,urrogate/Tracer Recovery Test
Alphaspec Th, Liquid "As Received"
MDC
443
613
350
194
22.4
403
343
278
rhorium-229 Tracer
3arium Carrier
Jranium-232 Tracer
GFPC,Total Alpha Radium, Liquid "As Received"
U-233/234,U-235/236 and U-238 "As Received"
IJotes:
RL
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Analyst
=:ounting Uncertainty is calculated at the 68% confidence level (I-sigma).
Project:
Client ID:
DNMI00107
DNMI001
Units PF DF Analyst Date Time Batch Method
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
Date
Result
JXB7 09/11/19 1927 1914167
AXM6 09/12/19 1658 1914172
MXH8 09/12/19 1034 1914039
JXB7 09/11/19 1927 1914171
Time Prep Batch
1912341
Anal st Comments
Nominal Recove %
82.3
IOI
95
Acceptable Limits
(15%-125%)
(25%-125%)
(15%-125%)
2
3
4
,RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Page 43 of 50 SDG: 488668 Revl
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company :
Address:
Contact:
Project:
Client Sample ID:
Sample ID:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy W einel
Tailings 2019 Characterization
Cell4B LDS
488668007
Parameter Qualifier Result Uncertainty MDC
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
RL
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 44 of 50 SDG: 488668 Revl
Project:
Client ID:
DNMI00107
DNMI001
Units PF DF Analyst Date Time Batch Method
EI\ERGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-008
Client Sample ID: Cell 65
Analyses Result Units Qualifiers
MAJOR IONS
Alkalinity, Total as CaC03 ND mg/L
Carbonate as C03 ND mg/L
Bicarbonate as HC03 ND mg/L
Chloride 19300 mg/L D
Fluoride 2980 mg/L D
Sulfate 169000 mg/L D
PHYSICAL PROPERTIES
Conductivity@ 25 C 118000 umhos/cm E
pH 1.13 s.u. H
pH Measurement Temp 18 oc
Solids, Total Dissolved TDS @ 180 C 255000 mg/L D
NUTRIENTS
Nitrogen, Nitrate+Nitrite as N 114 mg/L D
Nitrogen, Ammonia as N 12000 mg/L D
METALS, DISSOLVED
Arsenic 230 mg/L
Beryllium 0.90 mg/L
Cadmium 4.8 mg/L
Calcium 620 mg/L
Chromium 12 mg/L
Cobalt 60 mg/L
Copper 1500 mg/L
Iron 7800 mg/L
Lead 22 mg/L
Magnesium 7000 mg/L
Manganese 470 mg/L
Mercury 3.2 ug/L
Molybdenum 110 mg/L
Nickel 90 mg/L
Potassium 1900 mg/L
Selenium 7.9 mg/L
Silver 0.69 mg/L
Sodium 21000 mg/L
Thallium 0.13 mg/L
Tin 0.46 mg/L
Uranium 77 mg/L
Vanadium 1300 mg/L
Zinc 490 mg/L
VOLATILE ORGANIC COMPOUNDS
Tetrahydrofuran ND ug/L
Report RL -Analyte reporting limit.
Definitions: QCL -Quality control limit.
D -RL increased due to sample matrix.
H -Analysis performed past recommended holding time.
MCU
RL QCL
5
5
5
100
50
400
5
0.01
2000
0.5
1000
1
0.06
0.06
20
1
0.2
4
6
0.4
6
0.5
0.2
0.6
0.6
10
0.6
0.2
10
0.2
0.2
0.1
10
2
35.0
Report Date: 11/25/19
Collection Date: 08/21/19 08:35
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
A2320 B 08/23/19 16: 11 / dmb
A2320 B 08/23/19 16: 11 / dmb
A2320 B 08/23/19 16: 11 / dmb
E300.0 09/10/19 15:06 / ljl
A4500-F C 08/26/19 18:59 / dmb
E300.0 09/10/19 15:06 / ljl
A2510 B 08/23/19 11 :55 I kjp
A4500-H B 08/23/19 11 :55 / kjp
A4500-H B 08/23/19 11 :55 / kjp
A2540 C 08/26/19 16: 11 / kjp
E353.2 08/27/19 13:57 / dmb
E350.1 08/26/19 18:16 / dmb
E200.7_8 10/26/19 07:25 / ta-a
E200.7 _8 10/26/19 07:25 / ta-a
E200.7_8 10/26/19 07:25 / ta-a
E200.7_8 10/26/19 07:25 / ta-a
E200.7 _8 10/26/19 07:25 I ta-a
E200.7 _8 10/26/19 07:25 / ta-a
E200.7_8 10/26/19 07:25 / ta-a
E200.7 _8 10/26/19 07:25 / ta-a
E200.7_8 10/26/19 07:25 I ta-a
E200.7_8 10/26/19 07:25 / ta-a
E200.7_8 10/26/19 07:25 I ta-a
E245.1 09/09/19 20:03 I ta-a
E200.7_8 10/26/19 07:25 I ta-a
E200.7_8 10/26/19 07:25 / ta-a
E200.7_8 10/26/19 07:25 I ta-a
E200.7 _8 10/26/19 07:25 / ta-a
E200.7_8 10/26/19 07:25 I ta-a
E200.7 _8 10/26/19 07:25 / ta-a
E200.7_8 10/26/19 07:25 / ta-a
E200.7_8 10/26/19 07:25 / ta-a
E200.7_8 10/26/19 07:25 / ta-a
E200.7_8 10/26/19 07:25 I ta-a
E200.7_8 10/26/19 07:25 I ta-a
SW8260B 09/03/19 16:57 I ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
E -Estimated value. Result exceeds the instrument upper
quantitation limit.
Page 40 of 172
EI\ERGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABO RA TORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 08:35
Lab ID: C 19081073-008 Date Received: 08/22/19
Client Sample ID: Cell 65 Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
VOLATILE ORGANIC COMPOUNDS
Acetone 30 ug/L 20 SW8260B 09/04/19 10:44 / dm
Acetonitrile 32 ug/L 20 SW8260B 09/04/19 10:44 / dm
Acrolein ND ug/L 20 SW8260B 09/04/19 10:44 / dm
Acrylonitrile ND ug/L 20 SW8260B 09/04/19 10:44 / dm
Benzene ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
Bromobenzene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Bromochloromethane ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
Bromodichloromethane ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
Bromoform ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
Bromomethane ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
n-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
sec-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
tert-Butylbenzene ND ug/L 1.0 SWS260B 09/04/19 10:44 I dm
Carbon disulfide ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
Carbon tetrachloride ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
Chlorobenzene ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
Chlorodibromomethane ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Chloroethane 1.6 ug/L 1.0 SWS260B 09/04/19 10:44 / dm
2-Chloroethyl vinyl ether ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
Chloroform 6.9 ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Chloromethane 2.4 ug/L 1.0 SW8260B 09/04/19 10:44 I dm
2-Chlorotoluene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
4-Chlorotoluene ND ug/L 1.0 SWS260B 09/04/19 10:44 I dm
1,2-Dibromo-3-chloropropane ND ug/L 2.0 SW8260B 09/04/19 10:44 / dm
1,2-Dibromoethane ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
Dibromomethane ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
1,2-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
1,3-Dichlorobenzene ND ug/L 1.0 SWS260B 09/04/19 10:44 I dm
1,4-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
Dichlorodifluoromethane ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
1, 1-Dichloroethane ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
1,2-Dichloroethane ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
1, 1-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
cis-1,2-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
trans-1,2-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
1,2-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
1,3-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
2,2-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
1, 1-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
cis-1,3-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
trans-1,3-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Ethylbenzene ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
Hexachlorobutadiene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
Page 41 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 08:35
Lab ID: C 19081073-008 Date Received: 08/22/19
Client Sample ID: Cell 65 Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
VOLATILE ORGANIC COMPOUNDS
2-Hexanone ND ug/L 20 SW8260B 09/04/19 10:44 / dm
lodomethane ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
lsopropylbenzene ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
p-lsopropyltoluene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Methyl tert-butyl ether (MTBE) ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Methyl ethyl ketone 10 ug/L J 20 SW8260B 09/04/19 10:44 / dm
Methyl isobutyl ketone ND ug/L 20 SW8260B 09/04/19 10:44 / dm
Methylene chloride ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
Naphthalene ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
n-Propylbenzene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Styrene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
1, 1, 1,2-Tetrachloroethane ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
1, 1,2,2-Tetrachloroethane ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Tetrachloroethene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Toluene ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
1,2,3-Trichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
1,2,4-Trichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
1, 1, 1-Trichloroethane ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
1, 1,2-Trichloroethane ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Trichloroethene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Trichlorofluoromethane ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
1,2,3-Trichloropropane ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
1,2,4-Trimethylbenzene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
1,3,5-Trimethylbenzene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Vinyl acetate ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Vinyl chloride ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
m+p-Xylenes ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
a-Xylene ND ug/L 1.0 SW8260B 09/04/19 10:44 / dm
Xylenes, Total ND ug/L 1.0 SW8260B 09/04/19 10:44 I dm
Surr: 1,2-Dichloroethane-d4 127 %REC 70-130 SW8260B 09/04/19 10:44 I dm
Surr: Dibromofluoromethane 118 %REC 70-130 SW8260B 09/04/19 10:44 / dm
Surr: p-Bromofluorobenzene 96.0 %REC 70-130 SW8260B 09/04/19 10:44 / dm
Surr: Toluene-dB 83.0 %REC 70-130 SW8260B 09/04/19 10:44 / dm
SEMI-VOLATILE ORGANIC COMPOUNDS
1,2,4-Trichlorobenzene ND ug/L H 10 SW8270C 09/12/19 23:4 7 I ta-a
1,2-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 23:4 7 I ta-a
1,3-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 23:47 I ta-a
1,4-Dichlorobenzene ND ug/L H 10 SW8270C 09/12/19 23:47 I ta-a
1-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 23:47 I ta-a
2,4,5-Trichlorophenol ND ug/L H 10 SW8270C 09/12/19 23:47 I ta-a
2,4,6-Trichlorophenol 5.2 ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
2,4-Dichlorophenol ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time. J -Estimated value. The analyte was present but less
than the reporting limit.
Page 42 of 172
EI\ERGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/25/19
Project: Annual Tails 2019 Collection Date: 08/21/19 08:35
Lab ID: C19081073-008 Date Received: 08/22/19
Client Sample ID: Cell 65 Matrix: Aqueous
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
SEMI-VOLATILE ORGANIC COMPOUNDS
2,4-Dimethylphenol ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
2,4-Dinitrophenol ND ug/L H 50 SW8270C 09/12/19 23:47 I ta-a
2,4-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
2,6-Dinitrotoluene ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
2-Chloronaphthalene ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
2-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 23:47 I ta-a
2-Methylnaphthalene ND ug/L H 10 SW8270C 09/12/19 23:47 I ta-a
2-Nitrophenol ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
3,3 · -Dichlorobenzidine ND ug/L H 49 SW8270C 09/12/19 23:47 I ta-a
4,6-Dinitro-2-methylphenol ND ug/L H 50 SW8270C 09/12/19 23:4 7 / ta-a
4-Bromophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
4-Chloro-3-methylphenol ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
4-Chlorophenol ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
4-Chlorophenyl phenyl ether ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
4-Nitrophenol ND ug/L H 50 SW8270C 09/12/19 23:47 / ta-a
Acenaphthene ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
Acenaphthylene ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
Anthracene ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
Azobenzene ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
Benzidine ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
Benzo(a)anthracene ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
Benzo(a)pyrene ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
Benzo(b)fluoranthene ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
Benzo(g, h,i)perylene ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
Benzo(k)fluoranthene ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
bis(-2-chloroethoxy)Methane ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
bis(-2-chloroethyl)Ether ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
bis(2-chloroisopropyl)Ether ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
bis(2-ethylhexyl)Phthalate ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
Butylbenzylphthalate ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
Chrysene ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
Di-n-butyl phthalate ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
Di-n-octyl phthalate ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
Dibenzo(a,h)anthracene ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
Diethyl phthalate ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
Dimethyl phthalate ND ug/L H 10 SW8270C 09/12/19 23:47 I ta-a
Fluoranthene ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
Fluorene ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
Hexachlorobenzene ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
Hexachlorobutadiene ND ug/L H 30 SW8270C 09/12/19 23:47 / ta-a
Hexachlorocyclopentadiene ND ug/L H 10 SW8270C 09/12/19 23:4 7 / ta-a
Hexachloroethane ND ug/L H 30 SW8270C 09/12/19 23:47 / ta-a
lndeno(1,2,3-cd)pyrene ND ug/L H 10 SW8270C 09/12/19 23:47 / ta-a
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
H -Analysis performed past recommended holding time.
Page 43 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-008
Client Sample ID: Cell 65
Analyses
SEMI-VOLATILE ORGANIC COMPOUNDS
lsophorone
m+p-Cresols
n-Nitroso-di-n-propylamine
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
o-Cresol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Qualifiers
H
H
H
H
H
H
H
H
H
H
H
H
H
H -Analysis performed past recommended holding time.
MCU
RL QCL
10
10
10
10
10
10
10
10
50
10
10
10
20
Report Date: 11/25/19
Collection Date: 08/21/19 08:35
DateReceived: 08/22/19
Matrix: Aqueous
Method Analysis Date / By
SW8270C 09/12/19 23:47 I ta-a
SW8270C 09/12/19 23:47 I ta-a
SW8270C 09/12/19 23:47 I ta-a
SW8270C 09/12/19 23:4 7 I ta-a
SW8270C 09/12/19 23:47 I ta-a
SW8270C 09/12/19 23:4 7 I ta-a
SW8270C 09/12/19 23:47 I ta-a
SW8270C 09/12/19 23:4 7 I ta-a
SW8270C 09/12/19 23:47 I ta-a
SW8270C 09/12/19 23:4 7 I ta-a
SW8270C 09/12/19 23:4 7 / ta-a
SW8270C 09/12/19 23:4 7 I ta-a
SW8270C 09/12/19 23:4 7 I ta-a
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 44 of 172
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Contact:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Project: Tailings 2019 Characterization
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Cell65
488668008
Water
21-AUG-19 08:35
24-AUG-19
Client
Qualifier Result -----------'---Parameter
fazardous Waste
\STM D 5057 Specific Gravity "As Received"
,pecific Gravity 1.15
The following Analytical Methods were performed:
----
DL
0.010
RL
0.100
------------------\.1 et hod Descri tion
ASTMD 5057
'fotes:
Project:
Client ID:
DNMI00107
DNMI001
Units PF DF Analyst Date Time Batch Method
none 1 VHI 08/30/19 1124 1913001
Anal st Comments
,RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Column headers are defined as follows:
OF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 22 of 50 SDG: 488668 Revl
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company:
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Contact:
Lakewood, Colorado 80228
Ms. Kathy Weinel
Project: Tailings 2019 Characterization
Client Sample ID: Cell 65
Sample ID: 488668008
Matrix: Water
Collect Date: 21-AUG-19 08:35
Receive Date: 24-AUG-19
Collector: Client
Parameter Qualifier Result Uncertainty
-Iigh Rad Testing
\.lphaspec Th, Liquid "As Received"
'horium-228 1500 +/-440
'horium-230 6.63E+05 +/-7300
:horium-232 5720 +/-695
]FPC, Total Alpha Radium, Liquid "As Received"
}ross Radium Alpha 3.98E+05 +/-3070
~ucas Cell, Ra226, liquid "As Received"
tadium-226 434 +/-31.1
J-233/234,U-235/236 and U-238 "As Received"
Jranium-233/234 25500 +/-1370
Jranium-235/236 1960 +/-434
Jranium-238 27700 +/-1430
[he following Prep Methods were performed:
vfethod Description
L-RAD-A-026 Laboratory Filtration
The following Analytical Methods were performed:
MDC
1080
846
698
219
23.9
614
433
404
RL
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
Analyst
Project:
Client ID:
DNMI00107
DNMIOOl
Units PF DF Analyst Date Time Batch Method
pCi/L JXB7 09/11/19 1927 1914167
pCi/L
pCi/L
pCi/L AXM6 09/12/19 1658 1914172 2
pCi/L MXH8 09/12/19 1108 1914039 3
pCi/L JXB7 09/11/19 1927 1914171 4
pCi/L
pCi/L
Date Time Prep Batch
1912341
\.1ethod DescriP.tio:..:.n:__ ___________________ ..!,A..,,,n,,.,a,.,.ly,_,,_s'-"-t--'=C'--"o'-"m~m=en'"'t"'-s __________ _
DOE EML HASL-300, Th-01-RC Modified
EPA 903.0
EPA 903.1 Modified
DOE EML HASL-300, U-02-RC Modified
;urrogate/Tracer Recovery Test
rhorium-229 Tracer
3arium Carrier
Jranium-232 Tracer
~otes:
Alphaspec Th, Liquid "As Received"
GFPC,Total Alpha Radium, Liquid "As Received"
U-233/234,U-235/236 and U-238 "As Received"
=::ounting Uncertainty is calculated at the 68% confidence level (I-sigma).
Result Nominal Recovery%
78.3
102
81.4
Acceptable Limits
(15%-125%)
(25%-125%)
(15%-125%)
;RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
he greater of either the adjusted MDL or the CRDL.
Page 45 of 50 SDG: 488668 Revl
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Certificate of Analysis
Report Date: September 17, 2019
Company :
Address:
Contact:
Project:
Client Sample ID:
Sample ID:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Tailings 2019 Characterization
Cell 65
488668008
Parameter Qualifier Result Uncertainty MDC
Column headers are defined as follows:
OF: Dilution Factor
DL: Detection Limit
Le/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
RL
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 46 of 50 SDG: 488668 Revl
Project:
Client ID:
DNMI00107
DNMI001
Units PF DF Analyst Date Time Batch Method
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686. 7175 • Helena, MT 877 .472.0711
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11 /25/19
Collection Date: 08/21/19 08:35
DateReceived: 08/22/19
Matrix: Trip Blank
Project: Annual Tails 2019
Lab ID: C 19081073-009
Client Sample ID: Trip Blank 10988
MCU
Analyses Result Units Qualifiers RL QCL Method Analysis Date / By
VOLATILE ORGANIC COMPOUNDS
Acetone ND ug/L 20 SW8260B 09/04/19 05:26 I dm
Acetonitrile ND ug/L 20 SW8260B 09/04/19 05:26 I dm
Acrolein ND ug/L 20 SW8260B 09/04/19 05:26 I dm
Acrylonitrile ND ug/L 20 SW8260B 09/04/19 05:26 I dm
Benzene ND ug/L 1.0 SW8260B 09/04/19 05:26 / dm
Bromobenzene ND ug/L 1.0 SW8260B 09/04/19 05:26 / dm
Bromochloromethane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
Bromodichloromethane ND ug/L 1.0 SW8260B 09/04/19 05:26 / dm
Bromoform ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
Bromomethane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
n-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
sec-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
tert-Butylbenzene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
Carbon disulfide ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
Carbon tetrachloride ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
Chlorobenzene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
Chlorodibromomethane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
Chloroethane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
2-Chloroethyl vinyl ether ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
Chloroform ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
Chloromethane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
2-Chlorotoluene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
4-Chlorotoluene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
1,2-Dibromo-3-chloropropane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
1,2-Dibromoethane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
Dibromomethane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
1,2-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
1,3-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
1,4-Dichlorobenzene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
Dichlorodifluoromethane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
1, 1-Dichloroethane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
1,2-Dichloroethane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
1, 1-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
cis-1,2-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
trans-1 ,2-Dichloroethene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
1,2-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
1,3-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
2,2-Dichloropropane ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
1, 1-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
cis-1 ,3-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
trans-1, 3-Dichloropropene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
Ethylbenzene ND ug/L 1.0 SW8260B 09/04/19 05:26 / dm
Hexachlorobutadiene ND ug/L 1.0 SW8260B 09/04/19 05:26 I dm
Report RL -Analyte reporting limit. MCL -Maximum contaminant level.
Definitions: QCL -Quality control limit. ND -Not detected at the reporting limit.
Page 45 of 172
EI\ERGY Trust our People. Trust our Data.
www encrgylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
LABO RA TORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Tails 2019
Lab ID: C 19081073-009
Client Sample ID: Trip Blank 10988
Analyses
VOLATILE ORGANIC COMPOUNDS
2-Hexanone
lodomethane
lsopropylbenzene
p-lsopropyltoluene
Methyl tert-butyl ether (MTBE)
Methyl ethyl ketone
Methyl isobutyl ketone
Methylene chloride
Naphthalene
n-Propylbenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetrach loroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m+p-Xylenes
a-Xylene
Xylenes, Total
Surr: 1,2-Dichloroethane-d4
Surr: Dibromofluoromethane
Surr: p-Bromofluorobenzene
Surr: Toluene-dB
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
105 %REC
100 %REC
90.0 %REC
92.0 %REC
Report Date: 11/25/19
Collection Date: 08/21/19 08:35
Date Received: 08/22/19
Matrix: Trip Blank
MCU
Qualifiers RL QCL Method Analysis Date / By
20 SW82608 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 I dm
20 SW8260B 09/04/19 05:26 / dm
20 SW8260B 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 / dm
1.0 SW8260B 09/04/19 05:26 / dm
1.0 SW8260B 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 / dm
1.0 SW8260B 09/04/19 05:26 / dm
1.0 SW8260B 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 / dm
1.0 SW8260B 09/04/19 05:26 / dm
1.0 SW8260B 09/04/19 05:26 / dm
1.0 SW8260B 09/04/19 05:26 / dm
1.0 SW8260B 09/04/19 05:26 I dm
1.0 SW82608 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 / dm
1.0 SW8260B 09/04/19 05:26 / dm
1.0 SW8260B 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 I dm
1.0 SW8260B 09/04/19 05:26 I dm
70-130 SW8260B 09/04/19 05:26 I dm
70-130 SW8260B 09/04/19 05:26 / dm
70-130 SW8260B 09/04/19 05:26 / dm
70-130 SW8260B 09/04/19 05:26 / dm
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 46 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.051
Gillette, WY 866.686. 7175 • Helena, MT 877.472.071
ANALYTICAL SUMMARY REPORT
November 25, 2019
Energy Fuels Resources (USA) Inc
225 Union Blvd Ste 600
Lakewood, CO 80228-1826
Work Order: C19081073
Project Name: Annual Tails 2019
Quote ID: C5645
Energy Laboratories, Inc. Casper WY received the following 9 samples for Energy Fuels Resources (USA) Inc on 8/22/2019
for analysis.
Lab ID Client Sample ID Collect Date Receive Date Matrix Test
C 19081073-001 Cell 1 08/21/19 08:35 08/22/19 Aqueous Metals by ICP/ICPMS, Dissolved
Acidity, Total as CaC03
Alkalinity
Conductivity
Mercury, Dissolved
Fluoride
Anions by Ion Chromatography
pH Check for H2S04 Preserved
lnorganics
Metals pH check by the Laboratory
FIRST
Nitrogen, Ammonia
Nitrogen, Nitrate + Nitrite
pH
Sample Filtering, Metals
Digestion, Mercury by CVAA
Solids, Total Dissolved
Separatory Funnel Liquid-Liquid Ext.
Semi-Volatile Organic Compounds
8260-Volatile Organic Compounds-
Short List
8260-Volatile Organic Compounds-
Extended List
C 19081073-002 Cell 2 Slimes 08/21/19 09:05 08/22/19 Aqueous Same As Above
C 19081073-003 Cell 3 08/21 /19 09:20 08/22/19 Aqueous Same As Above
C 19081073-004 Cell4A 08/21 /19 09 :40 08/22/19 Aqueous Same As Above
C 19081073-005 Ce114A LOS 08/21/19 09:45 08/22/19 Aqueous Same As Above
C 19081073-006 Ce114B 08/21/19 10:15 08/22/19 Aqueous Same As Above
C 19081073-007 Cell 4B LOS 08/21/1910:30 08/22/19 Aqueous Same As Above
C 19081073-008 Cell 65 08/21/19 08:35 08/22/19 Aqueous Same As Above
C 19081073-009 Trip Blank 10988 08/21/19 08:35 08/22/19 Trip Blank 8260-Volatile Organic Compounds-
Extended List
The analyses presented in this report were performed by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601,
unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC
Summary Report, or the Case Narrative. Any issues encountered during sample receipt are documented in the Work Order Receipt
Checklist.
The results as reported relate only to the item(s) submitted for testing. This report shall be used or copied only in its entirety. Energy
Laboratories, Inc. is not responsible for the consequences arising from the use of a partial report.
If you have any questions regarding these test results, please contact your Project Manager .
Page 1 of 172
EN:RGY
'
Report Approved By:
Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.051
Gillette, WY 888.688.7175 • Helena, MT 877.472.071
ANALYTICAL SUMMARY REPORT
rl~~ Project Manager
Digitally signed by
Tessa Parke
Date: 2019.11.25 13:4 7:40 -07:00
Page 2 of 172
EN:RGY . '
CLIENT:
Project:
Work Order:
~-Trust our People. Trust our Data.
~ www.energylab.com
Energy Fuels Resources (USA) Inc
Annual Tails 2019
C19081073
ORIGINAL SAMPLE SUBMITIAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4°C (±2°C)
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686. 7175 • Helena, MT 877.472.0711
Report Date: 11 /25/19
CASE NARRATIVE
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are
hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has
begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for
PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELi's certification coverage by visiting www.energylab.com
ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Tests associated with analyst identified as ELI-B were subcontracted to Energy Laboratories, 1120 S. 27th St., Billings, MT,
EPA Number MT00005.
Prep Comments for Sample C19081073-001 C, Test PRP-FIL T-MET: The prep hold time was exceeded by 0.0296 days. -
The sample fraction submitted for Dissolved Metals Analysis was received in the laboratory unfiltered.
Prep Comments for Sample C19081073-002C, Test PRP-FIL T-MET: The prep hold time was exceeded by 0.00876 days. -
The sample fraction submitted for Dissolved Metals Analysis was received in the laboratory unfiltered.
Prep Comments for Sample C19081073-003C, Test PRP-FIL T-MET: -The sample fraction submitted for Dissolved Metals
Analysis was received in the laboratory unfiltered.
Prep Comments for Sample C19081073-004C, Test PRP-FIL T-MET: -The sample fraction submitted for Dissolved Metals
Analysis was received in the laboratory unfiltered.
Prep Comments for Sample C19081073-005C, Test PRP-FIL T-MET: -The sample fraction submitted for Dissolved Metals
Analysis was received in the laboratory unfiltered.
Page 3 of 172
EN:RGY
CLIENT:
Project:
Work Order:
~-Trust our People. Trust our Data.
~ www.energylab.com
Energy Fuels Resources (USA) Inc
Annual Tails 2019
C19081073
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 888.686.7175 • Helena, MT 877.472.0711
Report Date: 11 /25/19
CASE NARRATIVE
Prep Comments for Sample C19081073-006C, Test PRP-FIL T-MET: -The sample fraction submitted for Dissolved Metals
Analysis was received in the laboratory unfiltered.
Prep Comments for Sample C19081073-00?C, Test PRP-FIL T-MET: -The sample fraction submitted for Dissolved Metals
Analysis was received in the laboratory unfiltered.
Prep Comments for Sample C19081073-008C, Test PRP-FILT-MET: The prep hold time was exceeded by 0.0296 days. -
The sample fraction submitted for Dissolved Metals Analysis was received in the laboratory unfiltered.
Page 4 of 172
.-." .......... LINKS ......... , ..
,
Review your project
results through
Tota -Access
llf.av:e a Questron 1
~
k
'The
Ex ert
, ....
I
\lislt us at':
www.testaniericalnc.com
.;; eurofins Environment Testing
TestAmerica
ANALYTICAL REPORT
Eurofins TestAmerica, Denver
4955 Yarrow Street
Arvada, CO 80002
Tel: [phone]
Laboratory Job ID: 280-12?755-1
Client Project/Site: 11 (e) Byproduct Material
For:
Energy Laboratories, Inc.
2393 North Salt Creek Highway
PO BOX 247
Casper, Wyoming 82601
Attn: Ms. Tessa Parke
Authorized for release by:
9/24/2019 8:52:19 AM
DiLea Bindel, Project Manager I
[phone]
d ilea. bindel@testamericai nc. com
The test results in this report meet all 2003 NELAC and 2009 TN/ requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
Page 47 of 172
I
Client: Energy Laboratories, Inc.
ProjecUSite: 11 (e) Byproduct Material
Laboratory Job ID: 280-127755-1
Table of Contents
Cover Page ............................................. . 1
Table of Contents ........................................ . 2
Definitions .............................................. . 3
Case Narrative .......................................... . 4
Detection Summary ....................................... . 6
Method Summary ........................................ . 9
Sample Summary ........................................ . 10
Client Sample Results ..................................... . 11
Surrogate Summary ...................................... . 31
QC Sample Results ....................................... . 32
QC Association .......................................... . 40
Chronicle ............................................... . 42
Certification Summary ..................................... . 47
Chain of Custody ......................................... . 49
Receipt Checklists ........................................ . 54
Page 2 of 54 Eurofins TestAme!t_c,~~enver
Page 4S/a:J<Ww19
I
I
~
~
Definitions/Glossary
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Job ID: 280-127755-1
Qualifiers
GC/MSVOA
Qualifier Qualifier Description
J Result is less than the---=Rc-L-cb-u.,--t g-r-e-ater than or equal to the MDL and the concentration is an approximate v alue.
GC/MS Semi VOA
Qualifier
D
H
J
X
Metals
Qualifier
-J -
Glossary
Abbreviation
C
%R
CFL
CNF
DER
Oil Fae
DL
DL, RA, RE, IN
DLC
EDL
LOO
LOQ
MDA
MDC
MDL
ML
NC
ND
PQL
QC
RER
RL
RPO
TEF
TEQ
Qualifier Description
LCS or LCSD is outside acceptance limits.
RPO of the LCS and LCSD exceeds the control limits
Sample results are obtained from a dilution; the surrogate or matrix spike recoveries reported are calculated from diluted samples.
Sample was prepped or analyzed beyond the specified holding time
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Surrogate is outside control limits
Qualifier Description
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis
Percent Recovery
Contains Free Liquid
Contains No Free Liquid
Duplicate Error Ratio (normalized absolute difference)
Dilution Factor
Detection Limit (DoD/DOE)
Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
Decision Level Concentration (Radiochemistry)
Estimated Detection Limit (Dioxin)
Limit of Detection (DoD/DOE)
Limit of Quantitation (DoD/DOE)
Minimum Detectable Activity (Radiochemistry)
Minimum Detectable Concentration (Radiochemistry)
Method Detection Limit
Minimum Level (Dioxin)
Not Calculated
Not Detected at the reporting limit (or MDL or EDL if shown)
Practical Quantitation Limit
Quality Control
Relative Error Ratio (Radiochemistry)
Reporting Limit or Requested Limit (Radiochemistry)
Relative Percent Difference, a measure of the relative difference between two points
Toxicity Equivalent Factor (Dioxin)
Toxicity Equivalent Quotient (Dioxin)
Eurofins TestAmerica, Denver
Page 3 of 54 Page 49 c9@tf2019
I
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Job ID: 280-127755-1
Case Narrative
Laboratory: Eurofins TestAmerica, Denver
Narrative
CASE NARRATIVE
Client: Energy Laboratories, Inc.
Project: 11 (e) Byproduct Material
Report Number: 280-127755-1
Job ID: 280-127755-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 8/28/2019 10:45 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperatures of the 3 coolers at receipt time were 2.5° C, 2.8° C and 7.6° C.
The following sample was received by the laboratory; however, it was not listed on the Chain-of-Custody (COC): M3-54865
(280-127755-25).The sample was logged per the information stated on the sample container.
The containers for the following samples requesting method 8270C were received at the laboratory outside the required temperature
criteria: C19081073-005D (280-127755-14), C19081073-006D (280-127755-17), C19081073-007D (280-127755-20) and
C 19081073-008D (280-127755-23).
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples C19081073-001F (280-127755-3), C19081073-002F (280-127755-6), C19081073-003F (280-127755-9), C19081073-004F
(280-127755-12), C19081073-005F (280-127755-15), C19081073-006F (280-127755-18), C19081073-007F (280-127755-21) and
C19081073-008F (280-127755-24) were analyzed for volatile organic compounds (GC-MS) in accordance with EPA SW-846 Method
82608. The samples were analyzed on 09/03/2019.
The following samples were diluted due to the nature of the sample matrix: C19081073-001F (280-127755-3), C19081073-002F
(280-127755-6), C 19081073-003F (280-127755-9), C 19081073-004F (280-127755-12), C 19081073-005F (280-127755-15),
C19081073-006F (280-127755-18), C19081073-007F (280-127755-21) and C19081073-008F (280-127755-24). Elevated reporting
limits (Rls) are provided. The samples were blue-green in color and had a "greasy" sheen to the water.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
SEMIVOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples C19081073-001D (280-127755-2), C19081073-002D (280-127755-5), C19081073-003D (280-127755-8), C19081073-004D
(280-127755-11), C19081073-005D (280-127755-14), C19081073-0060 (280-127755-17), C19081073-007D (280-127755-20) and
C19081073-008D (280-127755-23) were analyzed for semivolatile organic compounds (GC-MS) in accordance with EPA SW-846 Method
8270C. The samples were prepared on 08/29/2019 and analyzed on 09/12/2019 and 09/17/2019.
The following samples were diluted due to the nature of the sample matrix: C 19081073-0040 (280-127755-11) and C 19081073-006D
(280-127755-17). Elevated reporting limits (Rls) are provided.
The following samples formed emulsions during the extraction procedure: C19081073-001D (280-127755-2), C19081073-002D
Page 4 of 54 Eurofins TestAmerica, Denver
Page 50 <9~2019
I
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
J.!)b ID:_280-127755-1 (Continued)
Case Narrative
Laboratory: Eurofins TestAmerica, Denver (Continued)
Job ID: 280-127755-1
(280-127755-5), C 19081073-003D (280-127755-8), C 19081073-004D (280-127755-11 ), C 19081073-005D (280-127755-14 ),
C19081073-006D (280-127755-17), C19081073-007D (280-127755-20) and C19081073-008D (280-127755-23). The emulsions were
broken up using a pour back technique.
The laboratory was unable to preform the base extraction due to emulsion that did not allow the sample to separate sufficiently:
C19081073-001D (280-127755-2), C19081073-002D (280-127755-5), C19081073-003D (280-127755-8), C19081073-004D
(280-127755-11), C19081073-005D (280-127755-14), C19081073-006D (280-127755-17), C19081073-007D (280-127755-20) and
C19081073-008D (280-127755-23).
Due to the high density of the sample matrix (>1 .0 g/ml), the initial volumes used for the following samples deviated from the standard
procedure: C19081073-001D (280-127755-2), C19081073-004D (280-127755-11) and C19081073-008D (280-127755-23). The
reporting limits (Rls) have been adjusted proportionately.
The following samples were prepared outside of preparation holding time due to the samples being received on the last day of the
method holding time. As such, the laboratory had insufficient time to extract the samples in hold: C19081073-001 D (280-127755-2),
C 19081073-002D (280-127755-5), C 19081073-003D (280-127755-8), C 19081073-004D (280-127755-11), C 19081073-005D
(280-127755-14), C19081073-006D (280-127755-17), C19081073-007D (280-127755-20) and C19081073-008D (280-127755-23).
Due to matrix interference, the following samples failed the surrogate recovery criteria low: C19081073-004D (280-127755-11),
(280-127755-17), C 19081073-0010 (280-127755-2), C 19081073-008D (280-127755-23).
The laboratory control sample duplicate (LCSD) for preparation batch 280-469200 and analytical batch 280-470328 recovered outside
control limits for the following analytes: 1,2,4,5-Tetrachlorobenzene and 1, 1'-Biphenyl. 1,2,4,5-Tetrachlorobenzene and 1, 1 '-Biphenyl have
been identified as a poor performing analytes when analyzed using this method; therefore, re-extraction/re-analysis was not performed.
1,2,4-Trichlorobenzene, 1,2-Dichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, Hexachlorobutadiene and lndene failed the
recovery criteria low for LCS 280-469200/2-A. Several analytes failed the recovery criteria low for LCSD 280-469200/3-A. Pyridine
exceeded the LCS/LCSD RPD limit. Refer to the QC report for details. Due to expired holding times data was reported as is and flagged
appropriately.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
DISSOLVED MERCURY (CVAA)
Samples C19081073-001C (280-127755-1), C19081073-002C (280-127755-4), C19081073-003C (280-127755-7), C19081073-004C
(280-127755-10), C 19081073-005C (280-127755-13), C 19081073-006C (280-127755-16), C 19081073-007C (280-127755-19),
C19081073-008C (280-127755-22) and M3-54865 (280-127755-25) were analyzed for dissolved mercury (CVAA) in accordance with EPA
Method 245.1. The samples were prepared and analyzed on 09/09/2019.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Page 5 of 54
Eurofins TestAmerica, Denver
Page 51 c9@ti2019
I
Detection Summary
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Client Sample ID: C19081073-001C Lab Sample ID: 280-127755-1
Analyte Result Qualifier RL MDL Unit Dil Fae D Method Prep Type
Mercury 3.7 0.20 0.027 ug/L -~1 -245.1 Dissolved
Client Sample ID: C19081073-001 D Lab Sample ID: 280-127755-2 I
Analyte Result Qualifier RL MDL Unit Dil Fae D Method Prep Type
Hexadecane 85 H 10 0.35 ug/L --1 -8270C Total/NA
Client Sample ID: C19081073-001F Lab Sample ID: 280-127755-3
No Detections.
Client Sample ID: C19081073-002C Lab Sample ID: 280-127755-4
No Detections.
Client Sample ID: C19081073-002D Lab Sample ID: 280-127755-5
Analyte Result Qualifier RL MDL Unit Dil Fae D Method Prep Type
1,4-Dioxane 14 JH 18 0.65 ug/L 1 8270C Total/NA
2-Methylnaphthalene 11 H* 3.7 0.38 ug/L 8270C Total/NA
Bis(2-ethylhexyl) phthalate 1.1 JH 9.2 1.0 ug/L 8270C Total/NA
Dimethyl phthalate 1.5 JH 3.7 1.2 ug/L 8270C Total/NA
Naphthalene 5.3 H* 3.7 0.37 ug/L 8270C Total/NA
1-Methylnaphthalene 12 H* 3.7 0.32 ug/L 8270C Total/NA
Client Sample ID: C19081073-002F Lab Sample ID: 280-127755-6
No Detections.
Client Sample ID: C19081073-003C Lab Sample ID: 280-127755-7
Analyte Result Qualifier RL MDL Unit Dil Fae D Method Prep Type
Mercury 0.20 0.20 0.027 ug/L --1 -245.1 Dissolved
Client Sample ID: C19081073-003D Lab Sample ID: 280-127755-8
Analyte Result Qualifier RL MDL Unit Dil Fae D Method Prep Type
Benzyl alcohol 8.0 J H 9.0 0.31 ug/L --1 -8270C Total/NA
------------------Client Sample ID: C19081073-003F Lab Sample ID: 280-127755-9
No Detections.
Client Sample ID: C19081073-004C Lab Sample ID: 280-127755-10
Analyte Result Qualifier RL MDL Unit Dil Fae D Method Prep Type
Mercury 2.1 0.20 0.027 ug/L --1 -245.1 Dissolved
Client Sample ID: C19081073-004D Lab Sample ID: 280-127755-11
Analyte Result Qualifier RL MDL Unit Dil Fae D Method Prep Type
Anthracene 1.2 JH 3.7 0.99 ug/L --1 -8270C Total/NA
Hexadecane -DL 320 H 37 1.3 ug/L 4 8270C Total/NA
Clie"!_t Sample ID: C19081073-004F Lab Sample ID: 280-127755-12
No Detections.
This Detection Summary does not include radiochemical test results.
Eurofins TestAmerica, Denver
Page 6 of 54 Page 52 <9/Q.ii/2019
Detection Summary
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 ( e) Byproduct Material
Client Sample ID: C19081073-005C Lab Sample ID: 280-127755-13
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Mercury --:a 0.20 0.027 ug/L 1 245.1 Dissolved
Client Sample ID: C19081073-005D Lab Sample ID: 280-127755-14 I
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Bis(2-ethylhexyl) phthalate 1.1 JH 9.2 1.0 ug/L --1 8270C Total/NA
Client Sample ID: C19081073-005F Lab Sample ID: 280-127755-15
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Tetrahydrofuran ---1-6 J 35 10 ug/L 5 -8260B Total/NA
Client Sample ID: C19081073-006C Lab Sample ID: 280-127755-16
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Mercury 0.46 0.20 0.027 ug/L --1 -245.1 Dissolved
Client Sample ID: C19081073-006D Lab Sample ID: 280-127755-17
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Anthracene 1.7 JH 3.5 0.94 ug/L --1 8270C Total/NA
Hexadecane -DL 190 H 35 1.2 ug/L 4 8270C Total/NA
Client Sample ID: C19081073-006F Lab Sample ID: 280-127755-18
No Detections.
Client Sample ID: C19081073-007C Lab Sample ID: 280-127755-19
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Mercury 0.11 J 0.20 0.027 ug/L 1 245.1 Dissolved
Client Sample ID: C19081073-007D Lab Sample ID: 280-127755-20
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Bis(2-ethylhexyl) phthalate 16 H 9.1 1.0 ug/L --1 -8270C Total/NA
3-Methylphenol 0.42 JH 9.1 0.36 ug/L 8270C Total/NA
Total Cresols 0.42 JH 9.1 0.36 ug/L 8270C Total/NA
Client Sample ID: C19081073-007F Lab Sample ID: 280-127755-21
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Tetrahydrofuran 53 35 10 ug/L ---5 -8260B Total/NA
Client Sample ID: C19081073-008C Lab Sample ID: 280-127755-22
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Mercury 3.2 0.20 0.027 ug/L --1 -245.1 Dissolved
Client Sample ID: C19081073-008D La_!> Sample ID: 280-127755-23 -~-
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
2,4,6-Trichlorophenol 5.2 JH 9.9 0.73 ug/L --1 -8270C Total/NA
Hexadecane 91 H 9.9 0.35 ug/L 1 8270C Total/NA
This Detection Summary does not include radiochemical test results.
Eurofins TestAmerica, Denver
Page 7 of 54 Page 53 c9/21t/2019
Client: Energy Laboratories, Inc.
ProjecUSite: 11 (e) Byproduct Material
Client Sample ID: C19081073-008F
No Detections.
Client Sample ID: M3-54865
No Detections.
Detection Summary
This Detection Summary does not include radiochemical test results.
Page 8 of 54
Job ID: 280-127755-1
Lab Sample ID: 280-127755-24
Lab Sample ID: 280-127755-25
I
Eurofins TestAmerica, Denver
Page 54 <912412019
Method Summary
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Method
82608
8270C
245.1
245.1
3510C
50308
Method Description
Volatile Organic Compounds (GC/MS)
Semivolatile Organic Compounds (GC/MS)
Mercury -Dissolved
Preparation, Mercury
Liquid-Liquid Extraction (Separatory Funnel)
Purge and Trap
Protocol References:
EPA= US Environmental Protection Agency
Job ID: 280-127755-1
Protocol Laboratory
SW846 TAL DEN
SW846 TAL DEN
EPA TALDEN
EPA TAL DEN
SW846 TAL DEN
SW846 TAL DEN
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL DEN= Eurofins TestAmerica, Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
Eurofins TestAmerica, Denver
Page 9 of 54 Page 55 <9/Q.it/2019
I
Sample Summary
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
ProjecUSite: 11 (e) Byproduct Material
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
280-1277 55-1 C19081073-001C Water 08/21/19 08:35 08/28/19 10:45
280-127755-2 C 19081073-0010 Water 08/21/19 08:35 08/28/19 10:45
280-127755-3 C19081073-001 F Water 08/21/19 08:35 08/28/19 10:45
280-127755-4 C 19081 073-002C Water 08/21/19 09:05 08/28/19 10:45
280-127755-5 C19081073-002D Water 08/21/19 09:05 08/28/19 10:45
280-127755-6 C 19081073-002F Water 08/21/19 09:05 08/28/19 10:45
280-127755-7 C 19081073-003C Water 08/21/19 09:20 08/28/19 10:45 I 280-127755-8 C 19081073-003D Water 08/21/19 09:20 08/28/19 10:45
280-1277 55-9 C 19081073-003F Water 08/21/19 09:20 08/28/19 10:45
280-127755-10 C 19081 073-004C Water 08/21 /19 09:40 08/28/19 10:45
280-127755-11 C 19081073-004D Water 08/21/19 09:40 08/28/19 10:45
280-127755-12 C19081073-004F Water 08/21/19 09:40 08/28/19 10:45
280-127755-13 C 19081 073-005C Water 08/21/19 09:45 08/28/19 10:45
280-127755-14 C 19081 073-005D Water 08/21/19 09:45 08/28/19 10:45
280-127755-15 C 19081073-005F Water 08/21/19 09:45 08/28/19 10:45
280-127755-16 C19081073-006C Water 08/21/1910:15 08/28/19 10:45
280-127755-17 C19081073-006D Water 08/21/19 10:15 08/28/19 10:45
280-127755-18 C19081073-006F Water 08/21/1910:15 08/28/19 10:45
280-127755-19 C19081073-007C Water 08/21/1910:30 08/28/19 10:45
280-127755-20 C19081073-007D Water 08/21/19 10:30 08/28/19 10:45
280-1277 55-21 C19081073-007F Water 08/21/19 10:30 08/28/19 10:45
280-127755-22 C 19081073-008C Water 08/21/19 08:35 08/28/19 10:45
280-127755-23 C 19081073-008D Water 08/21/19 08:35 08/28/19 10:45
280-127755-24 C19081073-008F Water 08/21/19 08:35 08/28/19 10:45
280-127755-25 M3-54865 Water 08/23/19 11 :20 08/28/19 10:45
Eurofins TestAmerica, Denver
Page 10 of 54 Page 56 c9/002019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 ( e) Byproduct Material
Method: 82608 -Volatile Organic Compounds (GC/MS)
Client Sample ID: C19081073-001F Lab Sample ID: 280-127755-3
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/1910:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
T etrahydrofuran ND ~~ 10 ug/L 09/03/19 14:28 --5
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fae
1,2-Dichloroethane-d4 (Surr) 97 70-127 09/03/19 14:28 ---5
Toluene-dB (Surr) 96 80-125 09/03/19 14:28 5
4-Bromofluorobenzene (Surr) 93 78-120 09/03/19 14:28 5 I Dibromofluoromethane (Surr) 99 77-120 09/03/19 14:28 5
Client Sample ID: C19081073-002F Lab Sample ID: 280-127755-6
Date Collected: 08/21/19 09:05 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Tetrahydrofuran ND 35 10 ug/L 09/03/19 14:50 --5
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fae
1,2-Dichloroethane-d4 (Surr) 96 70-127 09/03/19 14:50 ---5
Toluene-dB (Surr) 96 80-125 09/03/19 14:50 5
4-Bromofluorobenzene (Surr) 95 78-120 09/03119 14:50 5
Dibromofluoromethane (Surr) 99 77-120 09/03/19 14:50 5
Client Sample ID: C19081073-003F Lab Sample ID: 280-127755-9
Date Collected: 08/21/19 09:20 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Tetrahydrofuran --l'Ji5 35 10 ug/L 09/03/19 15: 11 ---5
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fae
1,2-Dichloroethane-d4 (Surr) 97 70-127 09/03/19 15:11 5
Toluene-dB (Surr) 95 80-125 09/03/19 15: 11 5
4-Bromofluorobenzene (Surr) 93 78-120 09/03/19 15:11 5
Dibromofluoromethane (Surr) 100 77 -120 09/03/19 15:11 5
Client Sample ID: C19081073-004F Lab Sample ID: 280-127755-12
Date Collected: 08/21/19 09:40 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Tetrahydrofuran ND 35 10 ug/L 09/03/19 15:32 ~
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fae
1,2-Dichloroethane-d4 (Surr) 98 70-127 09/03119 15:32 --5
Toluene-dB (Surr) 96 80-125 09/03119 15:32 5
4-Bromof/uorobenzene (Surr) 93 78-120 09/03/19 15:32 5
Dibromofluoromethane (S urr) 99 77 -120 09/03119 15:32 5
Client Sample ID: C19081073-005F Lab Sample ID: 280-127755-15
Date Collected: 08/21/19 09:45 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Tetrahydrofuran 16 J 35 10 ug/L 09/03/19 15:53 --5
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fae
1,2-Dichloroethane-d4 (Surr) 97 70-127 09/03119 15:53 ---5
Eurofins TestAmerica, Denver
Page 11 of 54 Page 57 c9~2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
ProjecUSite: 11 (e) Byproduct Material
Method: 82608 -Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: C19081073-005F Lab Sample ID: 280-127755-15
Date Collected: 08/21/19 09:45 Matrix: Water
Date Received: 08/28/19 10:45
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
Toluene-dB (Surr) 98 80-125 09/03/19 15:53 ---5
4-Bromofluorobenzene (Surr) 93 78 -120 09/03/19 15:53 5
Dibromofluoromethane (Surr) 98 77-120 09/03/19 15:53 5
Client Sample ID: C19081073-006F Lab Sample ID: 280-127755-18 I Date Collected: 08/21 /19 10: 15 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Tetrahydrofuran ND 35 10 ug/L 09/03/19 16:14 ---5
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
1,2-Diehloroethane-d4 (Surr) 99 70-127 09/03119 16:14 ---5
Toluene-dB (Surr) 96 80-125 09103/19 16:14 5
4-Bromofluorobenzene (Surr) 93 78-120 09103/19 16:14 5
Dibromofluoromethane (Surr) 98 77-120 09/03/19 16:14 5
Client Sample ID: C19081073-007F Lab Sample ID: 280-127755-21
Date Collected: 08/21/19 10:30 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Tetrahydrofuran 53 35 10 ug/L 09103/19 16:35 5
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
1,2-Diehloroethane-d4 (Surr) 98 70-127 09/03119 16:35 ---5
Toluene-dB (Surr) 97 80-125 09103/19 16:35 5
4-Bromofluorobenzene (Surr) 93 78-120 09/03/19 16:35 5
Dibromofluoromethane (Surr) 100 77-120 09103/19 16:35 5
Client Sample ID: C19081073-008F Lab Sample ID: 280-127755-24
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Tetrahyd rofuran ND 35 ----:;a ug/L 09103119 16:57 ---5
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
1,2-Diehloroethane-d4 (Surr) 99 70-127 09103/19 16:57 ---5
Toluene-dB (Surr) 97 80-125 09/03/19 16:57 5
4-Bromofluorobenzene (Surr) 94 78-120 09/03/19 16:57 5
Dibromofluoromethane (Surr) 99 77-120 09/03119 16:57 5
Method: 8270C -Semivolatile Organic Compounds (GC/MS)
Client Sample ID: C19081073-001D Lab Sample ID: 280-127755-2
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
1, 1 '-Biphenyl ND H* 10 0.41 ugll 08/29/19 12:28 09112119 20:21 --1
1,2,4,5-Tetrachlorobenzene ND H* 10 0.24 ugll 08/29/19 12:28 09/12/19 20:21
1,2,4-Trichlorobenzene ND H* 5.0 0.37 ug/L 08/29/19 12:28 09/12/19 20:21
1,2-Dichlorobenzene ND H* 5.0 0.30 ug/L 08/29/19 12:28 09/12/19 20:21
1,3-Dichlorobenzene ND H* 10 2.0 ug/L 08/29/19 12:28 09/12/19 20:21
Eurofins TestAmerica, Denver
Page 12 of 54 Page 58 c910t/2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
ProjecUSite: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: C19081073-001 D Lab Sample ID: 280-127755-2
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
1,4-Dichlorobenzene --ND H* 5.0 --0.30 ug/L 08/29/19 12:28 09/12/1920:21 --1
1,4-Dioxane ND H 20 0.71 ug/L 08/29/19 12:28 09/12/19 20:21 1
2,4 ,6-Trichlorophenol ND H 10 0.74 ug/L 08/29/19 12:28 09/12/19 20:21
2,4-Dichlorophenol ND H 10 0.68 ug/L 08/29/19 12:28 09/12/19 20:21
2,2'-oxybis[1-chloropropane] ND H 10 0.42 ug/L 08/29/19 12:28 09/12/19 20:21
2,3,4,6-Tetrachlorophenol ND H 50 0.96 ug/L 08/29/19 12:28 09/12/19 20:21 I 2,4,5-Trichlorophenol ND H 10 0.52 ug/L 08/29/19 12:28 09/12/19 20:21
2,4-Dimethylphenol ND H 10 0.67 ug/L 08/29/19 12:28 09/12/19 20:21
2,4-Dinitrotoluene ND H 10 0.93 ug/L 08/29/19 12:28 09/12/19 20:21
2,6-Dinitrotoluene ND H 10 0.72 ug/L 08/29/19 12:28 09/12/19 20:21
2-Chloronaphthalene ND H • 4.0 0.46 ug/L 08/29/19 12:28 09/12/19 20:21
2-Chlorophenol ND H 10 0.43 ug/L 08/29/19 12:28 09/12/19 20:21
2-Methylnaphthalene ND H • 4.0 0.41 ug/L 08/29/19 12:28 09/12/19 20:21
2-Methylphenol ND H 10 0.56 ug/L 08/29/19 12:28 09/12/19 20:21
3 & 4 Methylphenol ND H 10 1.0 ug/L 08/29/19 12:28 09/12/19 20:21
2-Nitroaniline ND H 10 0.90 ug/L 08/29/19 12:28 09/12/19 20:21
2-Nitrophenol ND H 10 0.62 ug/L 08/29/19 12:28 09/12/19 20:21 1
3,3'-Dichlorobenzidine ND H 50 0.83 ug/L 08/29/19 12:28 09/12/19 20:21 1
3-Nitroaniline ND H 10 0.78 ug/L 08/29/19 12:28 09/12/19 20:21 1
4,6-Dinitro-2-methylphenol ND H 50 5.9 ug/L 08/29/19 12:28 09/12/19 20:21
4-Bromophenyl phenyl ether ND H 10 0.41 ug/L 08/29/19 12:28 09/12/19 20:21
4-Chloro-3-methylphenol ND H 10 0.45 ug/L 08/29/19 12:28 09/12/19 20:21
4-Chloroaniline ND H 10 0.56 ug/L 08/29/19 12:28 09/12/19 20:21
4-Chlorophenyl phenyl ether ND H 10 0.63 ug/L 08/29/19 12:28 09/12/19 20:21
4-Nitroaniline ND H 10 0.84 ug/L 08/29/19 12:28 09/12/19 20:21 1
4-Nitrophenol ND H 10 1.0 ug/L 08/29/19 12:28 09/12/19 20:21
Acenaphthene ND H 4.0 0.45 ug/L 08/29/19 12:28 09/12/19 20:21
Acenaphthylene ND H ' 4.0 0.50 ug/L 08/29/19 12:28 09/12/19 20:21
Acetophenone ND H 10 0.52 ug/L 08/29/19 12:28 09/12/19 20:21
Anthracene ND H 4.0 1.1 ug/L 08/29/19 12:28 09/12/19 20:21
Benzaldehyde ND H 10 0.53 ug/L 08/29/19 12:28 09/12/19 20:21
Benzo[a]pyrene ND H 4.0 0.64 ug/L 08/29/19 12:28 09/12/19 20 :21
Benzo[b]fluoranthene ND H 4.0 0.53 ug/L 08/29/19 12:28 09/12/19 20:21
Benzo[g,h,i]perylene ND H 4.0 0.79 ug/L 08/29/19 12:28 09/12/19 20:21
Benzo[k]fluoranthene ND H 4.0 0.56 ug/L 08/29/19 12:28 09/12/19 20:21
Benzo[a]anthracene ND H 4.0 0.58 ug/L 08/29/19 12:28 09/12/19 20:21
Bis(2-chloroethoxy)methane ND H 10 0.61 ug/L 08/29/19 12:28 09/12/19 20:21
Bis(2-chloroethyl)ether ND H 10 0.49 ug/L 08/29/19 12:28 09/12/19 20:21
Bis(2-ethylhexyl) phthalate ND H 10 1.1 ug/L 08/29/19 12:28 09/12/19 20:21
Butyl benzyl phthalate ND H 5.0 2.0 ug/L 08/29/1912:28 09/12/19 20:21
Caprolactam ND H 10 2.7 ug/L 08/29/19 12:28 09/12/19 20:21
Carbazole ND H 4.0 1.3 ug/L 08/29/19 12:28 09/12/19 20:21
Chrysene ND H 4.0 0.52 ug/L 08/29/19 12:28 09/12/19 20:21
Dibenz(a,h)anthracene ND H 4.0 0.65 ug/L 08/29/19 12:28 09/12/19 20:21
Di-n-butyl phthalate ND H 4.0 0.88 ug/L 08/29/19 12:28 09/12/19 20:21
Di-n-octyl phthalate ND H 5.0 1.6 ug/L 08/29/19 12:28 09/12/19 20:21
Dibenzofuran ND H 4.0 0.36 ug/L 08/29/19 12:28 09/12/19 20:21
Diethyl phthalate ND H 4.0 0.75 ug/L 08/29/19 12:28 09/12/19 20:21
Dimethyl phthalate ND H 4.0 1.3 ug/L 08/29/19 12:28 09/12/19 20:21
Eurofins TestAmerica, Denver
Page 13 of 54 Page 59 c9/0tl2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: C19081073-001D Lab Sample ID: 280-127755-2
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Fluoranthene ND H 4.0 --0.64 ug/L ___ 08/29/19 12:28 09/12/19 20:21 --1
Fluorene ND H 4.0 0.49 ug/L 08/29/19 12:28 09/12/19 20:21 1
Hexachlorobenzene ND H 10 0.96 ug/L 08/29/19 12:28 09/12/19 20:21
Hexachlorobutadiene ND H* 30 7.5 ug/L 08/29/19 12:28 09/12/19 20:21
Hexachloroethane ND H* 30 7.6 ug/L 08/29/19 12:28 09/12/19 20:21
lndeno[1,2,3-cd]pyrene ND H 5.0 1.6 ug/L 08/29/19 12:28 09/12/19 20:21 I lsophorone ND H 10 0.67 ug/L 08/29/19 12:28 09/12/19 20:21
N-Nitrosodi-n-propylamine ND H 10 0.56 ug/L 08/29/19 12:28 09/12/19 20:21
n-Nitrosodiphenylamine(as ND H 10 0.61 ug/L 08/29/19 12:28 09/12/19 20:21 1
diphenylamine)
Naphthalene ND H " 4.0 0.40 ug/L 08/29/19 12:28 09/12/19 20:21
Nitrobenzene ND H 10 0.43 ug/L 08/29/19 12:28 09/12/19 20:21
Pentachlorophenol ND H 50 5.5 ug/L 08/29/19 12:28 09/12/19 20:21
Phenanthrene ND H 4.0 0.28 ug/L 08/29/19 12:28 09/12/19 20:21
Phenol ND H 10 0.56 ug/L 08/29/19 12:28 09/12/19 20:21
Pyrene ND H 10 0.43 ug/L 08/29/19 12:28 09/12/19 20:21
1,3-Dinitrobenzene ND H 10 0.97 ug/L 08/29/19 12:28 09/12/19 20:21
1-Methylnaphthalene ND H * 4.0 0.35 ug/L 08/29/19 12:28 09/12/19 20:21
2,6-Dichlorophenol ND H 10 0.75 ug/L 08/29/19 12:28 09/12/19 20:21
Aniline ND H 10 0.88 ug/L 08/29/19 12:28 09/12/19 20:21
Azobenzene ND H 4.0 0.54 ug/L 08/29/19 12:28 09/12/19 20:21
Benzidine ND H 100 4.4 ug/L 08/29/19 12:28 09/12/19 20:21
Benzyl alcohol ND H 10 0.35 ug/L 08/29/19 12:28 09/12/19 20:21
Diphenylamine ND H 10 0.49 ug/L 08/29/19 12:28 09/12/19 20:21
Hexadecane 85 H 10 0.35 ug/L 08/29/19 12:28 09/12/19 20:21 1
N-Nitrosodimethylamine ND H 10 0.62 ug/L 08/29/19 12:28 09/12/19 20:21 1
Pyridine ND H * 20 5.0 ug/L 08/29/19 12:28 09/12/19 20:21
1,2-Diphenylhydrazine(as ND H 10 0.54 ug/L 08/29/19 12:28 09/12/19 20:21
Azobenzene)
3-Methylphenol ND H 10 0.40 ug/L 08/29/19 12:28 09/12/19 20:21
4-Methylphenol ND H 10 1.0 ug/L 08/29/19 12:28 09/12/19 20:21
Alachlor ND H 20 0.60 ug/L 08/29/19 12:28 09/12/19 20:21
Famphur ND H 100 0.80 ug/L 08/29/19 12:28 09/12/19 20:21
lndene ND H • 10 0.82 ug/L 08/29/19 12:28 09/12/19 20:21
Total Cresols ND H 10 0.40 ug/L 08/29/19 12:28 09/12/19 20:21
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fae
2-FTuorophenol 28 17 -71 08129/19 12:28 09112/19 20:21 ---1
Phenol-d5 26 10-52 08/29/19 12:28 09/12119 20:21 1
2, 4, 6-Tribromophenol 34 X 52-123 08/29/19 12:28 09/12119 20:21 1
2-Fluorobipheny/ 26 X 47-119 08/29/19 12:28 09/12119 20:21 1
Nitrobenzene-d5 36 X 45-113 08/29/19 12:28 09/12119 20:21 1
Terphenyl-d14 27 X 50-123 08/29/19 12:28 09/12/19 20:21 1
Client Sample ID: C19081073-002D Lab Sample ID: 280-127755-5
Date Collected: 08/21/19 09:05 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
1, 1 '-Biphenyl ND H* 9.2 0.38 ug/L 08/29/19 12:28 09/12/19 20:51 ---1
1,2 ,4 ,5-Tetrachlorobenzene ND H* 9.2 0.22 ug/L 08/29/19 12:28 09/12/19 20:51 1
Eurofins TestAmerica, Denver
Page 14 of 54 Page 60 c91M/2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: C19081073-002D Lab Sample ID: 280-127755-5
Date Collected: 08/21/19 09:05 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
1,2 ,4-Trichlorobenzene ND H* 4.6 0.34 ug/L 08/29/19 12:28 09/12/19 20:51 --1
1,2-Dichlorobenzene ND H* 4.6 0.28 ug/L 08/29/19 12:28 09/12/19 20:51
1,3-Dichlorobenzene ND H* 9.2 1.8 ug/L 08/29/19 12:28 09/12/19 20:51
1,4-Dichlorobenzene ND H* 4.6 0.27 ug/L 08/29/19 12:28 09/12/19 20:51
1,4-Dioxane 14 JH 18 0.65 ug/L 08/29/19 12:28 09/12/19 20:51
2,4,6-Trichlorophenol ND H 9.2 0.68 ug/L 08/29/19 12:28 09/12/19 20:51 I 2,4-Dichlorophenol ND H 9.2 0.63 ug/L 08/29/19 12:28 09/12/19 20:51
2,2'-oxybis[1-chloropropane] ND H 9.2 0.39 ug/L 08/29/19 12:28 09/12/19 20:51
2,3,4,6-Tetrachlorophenol ND H 46 0.89 ug/L 08/29/19 12:28 09/12/19 20:51
2,4,5-Trichlorophenol ND H 9.2 0.48 ug/L 08/29/19 12:28 09/12/19 20:51
2,4-Dimethylphenol ND H 9.2 0.62 ug/L 08/29/19 12:28 09/12/19 20:51
2,4-Dinitrotoluene ND H 9.2 0.86 ug/L 08/29/19 12:28 09/12/19 20:51
2,6-Dinitrotoluene ND H 9.2 0.66 ug/L 08/29/19 12:28 09/12/19 20:51
2-Chloronaphthalene ND H* 3.7 0.42 ug/L 08/29/19 12:28 09/12/19 20:51
2-Chlorophenol ND H 9.2 0.40 ug/L 08/29/19 12:28 09/12/19 20:51
2-Methylnaphthalene 11 H* 3.7 0.38 ug/L 08/29/19 12:28 09/12/19 20:51
2-Methylphenol ND H 9.2 0.52 ug/L 08/29/19 12:28 09/12/19 20:51
3 & 4 Methylphenol ND H 9.2 0.94 ug/L 08/29/19 12:28 09/12/19 20:51
2-Nitroaniline ND H 9.2 0.83 ug/L 08/29/19 12:28 09/12/19 20:51
2-Nitrophenol ND H 9.2 0.57 ug/L 08/29/19 12:28 09/12/19 20:51
3,3'-Dichlorobenzidine ND H 46 0.77 ug/L 08/29/19 12:28 09/12/19 20:51
3-Nitroaniline ND H 9.2 0.72 ug/L 08/29/19 12:28 09/12/19 20:51
4,6-Dinitro-2-methylphenol ND H 46 5.4 ug/L 08/29/19 12:28 09/12/19 20:51
4-Bromophenyl phenyl ether ND H 9.2 0.38 ug/L 08/29/19 12:28 09/12/19 20:51
4-Chloro-3-methylphenol ND H 9.2 0.41 ug/L 08/29/19 12:28 09/12/19 20:51
4-Chloroaniline ND H 9.2 0.52 ug/L 08/29/19 12:28 09/12/19 20:51
4-Chlorophenyl phenyl ether ND H 9.2 0.58 ug/L 08/29/19 12:28 09/12/19 20:51
4-Nitroaniline ND H 9.2 0.77 ug/L 08/29/19 12:28 09/12/19 20:51
4-Nitrophenol ND H 9.2 0.93 ug/L 08/29/19 12:28 09/12/19 20:51
Acenaphthene ND H 3.7 0.41 ug/L 08/29/19 12:28 09/12/19 20:51 1
Acenaphthylene ND H* 3.7 0.46 ug/L 08/29/19 12:28 09/12/19 20:51 1
Acetophenone ND H 9.2 0.48 ug/L 08/29/19 12:28 09/12/19 20:51 1
Anthracene ND H 3.7 0.99 ug/L 08/29/19 12:28 09/12/19 20:51
Benzaldehyde ND H 9.2 0.49 ug/L 08/29/19 12:28 09/12/19 20:51
Benzo[a]pyrene ND H 3.7 0.59 ug/L 08/29/19 12:28 09/12/19 20:51
Benzo[b]fluoranthene ND H 3.7 0.49 ug/L 08/29/19 12:28 09/12/19 20:51
Benzo[g,h,i]perylene ND H 3.7 0.73 ug/L 08/29/19 12:28 09/12/19 20:51
Benzo[k]fluoranthene ND H 3.7 0.52 ug/L 08/29/19 12:28 09/12/19 20:51
Benzo[a]anthracene ND H 3.7 0.53 ug/L 08/29/19 12:28 09/12/19 20:51
Bis(2-chloroethoxy)methane ND H 9.2 0.56 ug/L 08/29/19 12:28 09/12/19 20:51
Bis(2-chloroethyl)ether ND H 9.2 0.45 ug/L 08/29/19 12:28 09/12/19 20:51
Bis(2-ethylhexyl) phthalate 1.1 JH 9.2 1.0 ug/L 08/29/19 12:28 09/12/19 20:51 1
Butyl benzyl phthalate ND H 4.6 1.8 ug/L 08/29/19 12:28 09/12/19 20:51 1
Caprolactam ND H 9.2 2.5 ug/L 08/29/19 12:28 09/12/19 20:51 1
Carbazole ND H 3.7 1.2 ug/L 08/29/19 12:28 09/12/19 20:51
Chrysene ND H 3.7 0.48 ug/L 08/29/19 12:28 09/12/19 20:51
Dibenz(a,h)anthracene ND H 3.7 0.60 ug/L 08/29/19 12:28 09/12/19 20:51
Di-n-butyl phthalate ND H 3.7 0.81 ug/L 08/29/19 12:28 09/12/19 20:51
Di-n-octyl phthalate ND H 4.6 1.5 ug/L 08/29/19 12:28 09/12/19 20:51
Eurofins TestAmerica, Denver
Page 15 of 54 Page 61 c9/0t/2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: C19081073-002D Lab Sample ID: 280-127755-5
Date Collected: 08/21/19 09:05 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Dibenzofuran ~ -H-----3.7 0.33 ug/L 08/29/19 12:28 09/12/19 20:51 ---1
Diethyl phthalate ND H 3.7 0.69 ug/L 08/29/19 12:28 09/12/19 20:51 1
Dimethyl phthalate 1.5 JH 3.7 1.2 ug/L 08/29/19 12:28 09/12/19 20:51
Fluoranthene ND H 3.7 0.59 ug/L 08/29/19 12:28 09/12/19 20:51
Fluorene ND H 3.7 0.45 ug/L 08/29/19 12:28 09/12/19 20:51
Hexachlorobenzene ND H 9.2 0.89 ug/L 08/29/19 12:28 09/12/19 20:51 I Hexachlorobutadiene ND H* 28 6.9 ug/L 08/29/19 12:28 09/12/19 20:51
Hexachloroethane ND H* 28 7.0 ug/L 08/29/19 12:28 09/12/19 20:51
lndeno[1,2,3-cd]pyrene ND H 4.6 1.5 ug/L 08/29/19 12:28 09/12/19 20:51
lsophorone ND H 9.2 0.62 ug/L 08/29/19 12:28 09/12/19 20:51
N-Nitrosodi-n-propylamine ND H 9.2 0.52 ug/L 08/29/19 12:28 09/12/19 20:51
n-Nitrosodiphenylamine(as ND H 9.2 0.56 ug/L 08/29/19 12:28 09/12/19 20:51
diphenylamine)
Naphthalene 5.3 H* 3.7 0.37 ug/L 08/29/19 12:28 09/12/19 20:51
Nitrobenzene ND H 9.2 0.40 ug/L 08/29/19 12:28 09/12/19 20:51
Pentachlorophenol ND H 46 5.1 ug/L 08/29/19 12:28 09/12/19 20:51
Phenanthrene ND H 3.7 0.26 ug/L 08/29/19 12:28 09/12/19 20:51
Phenol ND H 9.2 0.52 ug/L 08/29/19 12:28 09/12/19 20:51
Pyrene ND H 9.2 0.40 ug/L 08/29/19 12:28 09/12/19 20:51
1,3-Dinitrobenzene ND H 9.2 0.89 ug/L 08/29/19 12:28 09/12/19 20:51
1-Methylnaphthalene 12 H* 3.7 0.32 ug/L 08/29/19 12:28 09/12/19 20:51
2,6-Dichlorophenol ND H 9.2 0.69 ug/L 08/29/19 12:28 09/12/19 20:51
Aniline ND H 9.2 0.81 ug/L 08/29/19 12:28 09/12/19 20:51
Azobenzene ND H 3.7 0.50 ug/L 08/29/19 12:28 09/12/19 20:51
Benzidine ND H 92 4.1 ug/L 08/29/19 12:28 09/12/19 20:51
Benzyl alcohol ND H 9.2 0.32 ug/L 08/29/19 12:28 09/12/19 20:51
Diphenylamine ND H 9.2 0.45 ug/L 08/29/19 12:28 09/12/19 20:51
Hexadecane ND H 9.2 0.33 ug/L 08/29/19 12:28 09/12119 20:51
N-Nitrosodimethylamine ND H 9.2 0.57 ug/L 08/29/19 12:28 09/12/19 20:51
Pyridine ND H* 18 4.6 ug/L 08/29/19 12:28 09/12/19 20:51
1,2-Diphenylhydrazine(as ND H 9.2 0.50 ug/L 08/29/19 12:28 09/12/19 20:51
Azobenzene)
3-Methylphenol ND H 9.2 0.37 ug/L 08/29/19 12:28 09/12/19 20:51 1
4-Methylphenol ND H 9.2 0.94 ug/L 08/29/19 12:28 09/12/19 20:51
Alachlor ND H 18 0.55 ug/L 08/29/19 12:28 09/12/19 20:51
Famphur ND H 92 0.73 ug/L 08/29/19 12:28 09/12/19 20:51
lndene ND H • 9.2 0.76 ug/L 08/29/19 12:28 09/12/19 20:51
Total Cresols ND H 9.2 0.37 ug/L 08/29/19 12:28 09/12/19 20:51
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
2-Fluorophenol 46 17 -71 08/29/19 12:28 09112/19 20:51 ---1
Phenol-d5 35 10-52 08/29/19 12:28 09112/19 20:51 1
2, 4, 6-Tribromophenol 76 52-123 08129/19 12:28 09/12/19 20:51 1
2-Fluorobiphenyl 60 47 -119 08/29/19 12:28 09/12/19 20:51 1
Nitrobenzene-d5 74 45_ 113 08/29/19 12:28 09/12/19 20:51 1
Terphenyl-d14 68 50-123 08/29/19 12:28 09/12119 20:51 1
Eurofins TestAmerica, Denver
Page 16 of 54 Page 62 c91'?.4'2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS)
Client Sample ID: C19081073-003D Lab Sample ID: 280-127755-8
Date Collected: 08/21/19 09:20 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
1, 1 '-Biphenyl ND H* 9.0 0.37 ug/L 08/29/1912:28 09/12/1921 :20 ---1
1,2,4,5-Tetrachlorobenzene ND H* 9.0 0.22 ug/L 08/29/19 12:28 09/12/19 21 :20
1,2,4-Trichlorobenzene ND H* 4.5 0.33 ug/L 08/29/19 12:28 09/12/19 21:20
1,2-0ichlorobenzene ND H* 4.5 0.27 ug/L 08/29/19 12:28 09/12/1921 :20
1,3-0ichlorobenzene ND H* 9.0 1.8 ug/L 08/29/19 12:28 09/12/1921 :20
1,4-Dichlorobenzene ND H* 4.5 0.26 ug/L 08/29/19 12:28 09/12/19 21 :20 I 1,4-Dioxane ND H 18 0.64 ug/L 08/29/19 12:28 09/12/1921 :20
2,4,6-Trichlorophenol ND H 9.0 0.66 ug/L 08/29/19 12:28 09/12/19 21 :20
2,4-Dichlorophenol ND H 9.0 0.61 ug/L 08129119 12:28 09112119 21 :20
2,2'-oxybis[1-chloropropane] ND H 9.0 0.38 ug/L 08129/19 12:28 09/12/19 21 :20
2,3,4,6-Tetrachlorophenol ND H 45 0.86 ug/L 08/29/19 12:28 09/12/19 21:20
2 ,4, 5-T richlorophenol ND H 9.0 0.47 ug/L 08/29119 12:28 09/12/1921 :20 1
2,4-Dimethylphenol ND H 9.0 0.60 ug/L 08/29/19 12:28 09/12/19 21 :20
2,4-Dinitrotoluene ND H 9.0 0.83 ug/L 08129119 12:28 09112/19 21:20
2,6-Dinitrotoluene ND H 9.0 0.64 ug/L 08/29/19 12:28 09/12/1921 :20
2-Chloronaphthalene ND H* 3.6 0.41 ug/L 08/29/19 12:28 09/12/1921 :20
2-Chlorophenol ND H 9.0 0.38 ug/L 08/29/19 12:28 09112119 21 :20
2-Methylnaphthalene ND H* 3.6 0.37 ug/L 08/29/19 12:28 09/12/1921 :20
2-Methylphenol ND H 9.0 0.50 ug/L 08/29/19 12:28 09/12/19 21 :20 1
3 & 4 Methylphenol ND H 9.0 0.91 ug/L 08129119 12:28 09/12119 21 :20 1
2-Nitroaniline ND H 9.0 0.81 ug/L 08/29/19 12:28 09/12/19 21 :20 1
2-Nitrophenol ND H 9.0 0.55 ug/L 08129/19 12:28 09112/19 21 :20
3,3'-Dichlorobenzidine ND H 45 0.74 ug/L 08/29/19 12:28 09/12/19 21 :20
3-Nitroaniline ND H 9.0 0.70 ug/L 08/29/19 12:28 09/12/19 21 :20
4,6-Dinitro-2-methylphenol ND H 45 5.2 ug/L 08/29/19 12:28 09/12/19 21 :20
4-Bromophenyl phenyl ether ND H 9.0 0.37 ug/L 08/29/19 12:28 09/12/1921 :20
4-Chloro-3-methylphenol ND H 9.0 0.40 ug/L 08/29/19 12:28 09/12/1921 :20 1
4-Chloroaniline ND H 9.0 0.50 ug/L 08/29/19 12:28 09/12/19 21 :20
4-Chlorophenyl phenyl ether ND H 9.0 0.56 ug/L 08/29/19 12:28 09/12/1921 :20
4-Nitroaniline ND H 9.0 0.75 ug/L 08/29/19 12:28 09/12/19 21 :20
4-Nitrophenol ND H 9.0 0.90 ug/L 08/29/19 12:28 09/12/19 21 :20
Acenaphthene ND H 3.6 0.40 ug/L 08/29/19 12:28 09/12/1921 :20
Acenaphthylene ND H* 3.6 0.45 ug/L 08/29/19 12:28 09/12119 21 :20 1
Acetophenone ND H 9.0 0.47 ug/L 08/29119 12 28 09/12/19 21 :20 1
Anthracene ND H 3.6 0.96 ug/L 08/29119 12:28 09/12119 21 :20
Benzaldehyde ND H 9.0 0.47 ug/L 08/29/19 12:28 09/12/19 21 :20
Benzo[a]pyrene ND H 3.6 0.57 ug/L 08/29/19 12:28 09/12/1921 :20 1
Benzo(b]fluoranthene ND H 3.6 0.47 ug/L 08129119 12:28 09/12119 21 :20 1
Benzo[g ,h, i]perylene ND H 3.6 0.71 ug/L 08129/19 12:28 09112/19 21 :20
Benzo[k]fluoranthene ND H 3.6 0.50 ug/L 08/29119 12:28 09112/19 21 :20 1
Benzo[a]anthracene ND H 3.6 0.52 ug/L 08/29/19 12:28 09/12/19 21 :20
Bis(2-chloroethoxy)methane ND H 9.0 0.55 ug/L 08/29/19 12:28 09/12/1921 :20
Bis(2-chloroethyl)ether ND H 9.0 0.44 ug/L 08/29/19 12:28 09/12/1921 :20
Bis(2-ethylhexyl) phthalate ND H 9.0 1.0 ug/L 08/29/19 12:28 09/12/19 21 :20
Butyl benzyl phthalate ND H 4.5 1.8 ug/L 08/29/19 12:28 09/12/19 21 :20
Caprolactam ND H 9.0 2.4 ug/L 08/29/19 12:28 09/12/19 21 :20
Carbazole ND H 3.6 1.2 ug/L 08/29/19 12:28 09/12/1921 :20 1
Chrysene ND H 3.6 0.47 ug/L 08/29119 12:28 09112119 21 :20 1
Dibenz(a,h)anthracene ND H 3.6 0.58 ug/L 08129/19 12:28 09/12/19 21 :20
Eurofins TestAmerica, Denver
Page 17 of 54 Page 63 .g/002019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: C19081073-003D Lab Sample ID: 280-127755-8
Date Collected: 08/21/19 09:20 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Di-n-butyl phthalate -ND H ----0.79 ug/L ---08/29/19 12:28 09/12/1921 :20 --1 3.6
Di-n-octyl phthalate ND H 4.5 1.4 ug/L 08/29/19 12:28 09/12/19 21 :20
Dibenzofuran ND H 3.6 0.32 ug/L 08/29/19 12:28 09/12/19 21 :20
Diethyl phthalate ND H 3.6 0.67 ug/L 08/29/19 12:28 09/12/19 21 :20
Dimethyl phthalate ND H 3.6 1.1 ug/L 08/29/19 12:28 09/12/1921 :20
Fluoranthene ND H 3.6 0.57 ug/L 08/29/19 12:28 09/12/19 21 :20 I Fluorene ND H 3.6 0.44 ug/L 08/29/19 12:28 09/12/19 21 :20
Hexachlorobenzene ND H 9.0 0.86 ug/L 08/29/19 12:28 09/12/1921 :20
Hexachlorobutadiene ND H* 27 6.7 ug/L 08/29/19 12:28 09/12/1921 :20 1
Hexachloroethane ND H" 27 6.8 ug/L 08/29/19 12:28 09/12/19 21 :20 1
lndeno[1,2,3-cd)pyrene ND H 4.5 1.5 ug/L 08/29/19 12:28 09/12/19 21 :20
lsophorone ND H 9.0 0.60 ug/L 08/29/19 12:28 09/12/1921 :20
N-Nitrosodi-n-propylamine ND H 9.0 0.50 ug/L 08/29/19 12:28 09/12/1921 :20
n-Nitrosodiphenylamine(as ND H 9.0 0.55 ug/L 08/29/19 12:28 09/12/19 21 :20
diphenylamine)
Naphthalene ND H * 3.6 0.36 ug/L 08/29/19 12:28 09/12/1921 :20
Nitrobenzene ND H 9.0 0.38 ug/L 08/29/19 12:28 09/12/19 21 :20
Pentachlorophenol ND H 45 4.9 ug/L 08/29/19 12:28 09/12/19 21 :20
Phenanthrene ND H 3.6 0.25 ug/L 08/29/19 12:28 09/12/19 21 :20
Phenol ND H 9.0 0.50 ug/L 08/29/19 12:28 09/12/1921 :20
Pyrene ND H 9.0 0.38 ug/L 08/29/19 12:28 09/12/19 21 :20
1,3-Dinitrobenzene ND H 9.0 0.87 ug/L 08/29/19 12:28 09/12/19 21 :20
1-Methylnaphthalene ND H * 3.6 0.31 ug/L 08/29/19 12:28 09/12/1921 :20
2,6-Dichlorophenol ND H 9.0 0.67 ug/L 08/29/19 12:28 09/12/1921 :20
Aniline ND H 9.0 0.79 ug/L 08/29/19 12:28 09/12/19 21 :20 1
Azobenzene ND H 3.6 0.48 ug/L 08/29/1912:28 09/12/1921 :20 1
Benzidine ND H 90 3.9 ug/L 08/29/19 12:28 09/12/19 21:20 1
Benzyl alcohol 8.0 JH 9.0 0.31 ug/L 08/29/19 12:28 09/12/1921 :20 1
Diphenylamine ND H 9.0 0.44 ug/L 08/29/19 12:28 09/12/19 21 :20 1
Hexadecane ND H 9.0 0.32 ug/L 08/29/19 12:28 09/12/1921 :20
N-Nitrosodimethylamine ND H 9.0 0.55 ug/L 08/29/19 12:28 09/12/1921 :20 1
Pyridine ND H * 18 4.5 ug/L 08/29/19 12:28 09/12/19 21 :20 1
1,2-Diphenylhydrazine(as ND H 9.0 0.48 ug/L 08/29/1912:28 09/12/19 21 :20
Azobenzene)
3-Methylphenol ND H 9.0 0.36 ug/L 08/29/19 12:28 09/12/19 21 :20
4-Methylphenol ND H 9.0 0.91 ug/L 08/29/19 12:28 09/12/19 21 :20
Alachlor ND H 18 0.54 ug/L 08/29/19 12:28 09/12/1921 :20 1
Famphur ND H 90 0.71 ug/L 08/29/19 12:28 09/12/19 21 :20 1
lndene ND H '• 9.0 0.73 ug/L 08/29/19 12:28 09/12/19 21 :20
Total Cresols ND H 9.0 0.36 ug/L 08/29/19 12:28 09/12/1921 :20 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
2-Fluorophenol 55 17 -71 08/29119 12:28 09/12119 21.·20 ---1
Phenol-d5 43 10-52 08/29/19 12.28 09/12119 21.20 1
2,4, 6-Tribromophenol 78 52-123 08/29119 12:28 09112/19 21:20 1
2-Fluorobiphenyl 63 47-119 08/29119 12:28 09112/19 21:20 1
Nitrobenzene-d5 75 45_ 113 08129/19 12:28 09/12119 21:20
Terphenyl-d14 72 50-123 08/29/19 12:28 09/12119 21:20 1
Eurofins TestAmerica, Denver
Page 18 of 54 Page 64 c9f24'2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS)
Client Sample ID: C19081073-004D Lab Sample ID: 280-127755-11
Date Collected: 08/21/19 09:40 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
1, 1 '-Biphenyl ND H* 9.3 0.38 ug/L 08/29/19 12:28 09/12/19 21 :49 1
1,2,4,5-Tetrachlorobenzene ND H* 9.3 0.23 ug/L 08/29/19 12:28 09/12/19 21 :49
1,2,4-Trichlorobenzene ND H* 4.6 0.34 ug/L 08/29/19 12:28 09/12/19 21 :49
1,2-Dichlorobenzene ND H* 4.6 0.28 ug/L 08/29/19 12:28 09/12/19 21 :49
1,3-Dichlorobenzene ND H* 9.3 1.9 ug/L 08/29/19 12:28 09112/19 21:49
1,4-Dichlorobenzene ND H* 4.6 0.27 ug/L 08/29/19 12:28 09/12/19 21 :49 I 1,4-Dioxane ND H 19 0.66 ug/L 08/29/19 12:28 09/12/1921 :49
2,4,6-Trichlorophenol ND H 9.3 0.69 ug/L 08/29/19 12:28 09/12/1921 :49
2,4-Dichlorophenol ND H 9.3 0.63 ug/L 08/29/19 12:28 09/12/1921 :49
2,2'-oxybis[1 -chloropropane] ND H 9.3 0.39 ug/L 08/29/19 12:28 09/12/19 21 :49
2,3,4,6-Tetrachlorophenol ND H 46 0.89 ug/L 08/29/19 12:28 09/12/19 21 :49
2,4,5-Trichlorophenol ND H 9.3 0.48 ug/L 08/29119 12:28 09/12/19 21 :49
2,4-Dimethylphenol ND H 9.3 0.62 ug/L 08/29/19 12:28 09/12/19 21 :49
2 ,4-Dinitrotoluene ND H 9.3 0.86 ug/L 08/29/19 12:28 09/12/19 21 :49
2,6-Dinitrotoluene ND H 9.3 0.67 ug/L 08/29/19 12:28 09/12/19 21 :49
2-Chloronaphthalene ND H * 3.7 0.43 ug/L 08/29/19 12:28 09/12/1921 :49
2-Chlorophenol ND H 9.3 0.40 ug/L 08/29/19 12:28 09/12/1921 :49
2-Methylnaphthalene ND H • 3.7 0.38 ug/L 08/29/19 12:28 09/12/1921 :49
2-Methylphenol ND H 9.3 0.52 ug/L 08/29/19 12:28 09/12/1921 :49
3 & 4 Methylphenol ND H 9.3 0.95 ug/L 08/29/19 12:28 09/12/19 21 :49 1
2-Nitroaniline ND H 9.3 0.84 ug/L 08/29/19 12:28 09/12/19 21 :49 1
2-Nitrophenol ND H 9.3 0.58 ug/L 08/29/19 12:28 09/12/19 21 :49
3,3'-Dichlorobenzidine ND H 46 0.77 ug/L 08/29/19 12:28 09/12/19 21 :49
3-Nitroaniline ND H 9.3 0.72 ug/L 08/29/19 12:28 09/12/19 21 :49
4,6-Dinitro-2-methylphenol ND H 46 5.4 ug/L 08/29/19 12:28 09/12/19 21 :49
4-Bromophenyl phenyl ether ND H 9.3 0.38 ug/L 08/29/19 12:28 09/12/1921 :49
4-Chloro-3-methylphenol ND H 9,3 0.42 ug/L 08/29/19 12:28 09/12/1921 :49
4-Chloroaniline ND H 9.3 0.52 ug/L 08/29/19 12:28 09/12/1921 :49
4-Chlorophenyl phenyl ether ND H 9.3 0.59 ug/L 08/29/19 12:28 09/12/1921 :49
4-Nitroaniline ND H 9.3 0.78 ug/L 08/29/19 12:28 09/12/19 21 :49
4-Nitrophenol ND H 9.3 0.94 ug/L 08/29/19 12:28 09/12/19 21 :49
Acenaphthene ND H 3.7 0.42 ug/L 08/29/19 12:28 09/12/19 21 :49
Acenaphthylene ND H* 3.7 0.46 ug/L 08/29/19 12:28 09/12/19 21 :49
Acetophenone ND H 9.3 0.48 ug/L 08/29/19 12:28 09/12/19 21 :49
Anthracene 1.2 JH 3.7 0.99 ug/L 08/29/19 12:28 09/12/19 21 :49
Benzaldehyde ND H 9.3 0.49 ug/L 08/29/19 12:28 09/12/1921 :49
Benzo[ a ]pyrene ND H 3.7 0.59 ug/L 08/29/19 12:28 09/12/1921 :49
Benzo[b]fluoranthene ND H 3.7 0.49 ug/L 08/29/19 12:28 09/12/19 21 :49
Benzo[g, h, i]perylene ND H 3.7 0.73 ug/L 08/29/19 12:28 09/12/19 21 :49
Benzo[k]fluoranthene ND H 3.7 0.52 ug/L 08/29/19 12:28 09/12/19 21 :49
Benzo[a]anthracene ND H 3.7 0.54 ug/L 08/29/1912:28 09/12/19 21 :49
Bis(2-chloroethoxy)methane ND H 9.3 0.57 ug/L 08/29/19 12:28 09/12/19 21 :49
Bis(2-chloroethyl)ether ND H 9.3 0.46 ug/L 08/29/19 12:28 09/12/19 21 :49
Bis(2-ethylhexyl) phthalate ND H 9.3 1.0 ug/L 08/29/19 12:28 09/12/1921 :49
Butyl benzyl phthalate ND H 4.6 1.9 ug/L 08/29/19 12:28 09/12/19 21 :49
Caprolactam ND H 9.3 2.5 ug/L 08/29/19 12:28 09/12/19 21 :49
Carbazole ND H 3.7 1.2 ug/L 08/29/19 12:28 09/12/1921 :49
Chrysene ND H 3.7 0.48 ug/L 08/29/19 12:28 09/12/19 21 :49
Dibenz(a,h)anthracene ND H 3.7 0.60 ug/L 08/29/19 12:28 09/12/19 21 :49
Eurofins TestAmerica, Denver
Page 19 of 54 Page 65 t9/0:tl2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
ProjecUSite: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: C19081073-004D Lab Sample ID: 280-127755-11
Date Collected: 08/21/19 09:40 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Di-n-butyl phthalate ND g-------0.82 ug/L --08/29/19 12:28 09/12/19 21 :49 --1 3.7
Di-n-octyl phthalate ND H 4.6 1.5 ug/L 08/29/19 12:28 09/12/19 21 :49
Dibenzofuran ND H 3.7 0.33 ug/L 08/29/19 12:28 09/12/1921 :49
Diethyl phthalate ND H 3.7 0.70 ug/L 08/29/19 12:28 09/12/19 21 :49
Dimethyl phthalate ND H 3.7 1.2 ug/L 08/29/19 12:28 09/12/1921 :49
Fluoranthene ND H 3.7 0.59 ug/L 08/29/19 12:28 09/12/19 21 :49 I Fluorene ND H 3.7 0.46 ug/L 08/29/19 12:28 09/12/19 21 :49
Hexachlorobenzene ND H 9.3 0.89 ug/L 08/29/19 12:28 09/12/19 21:49
Hexachlorobutadiene ND H" 28 7.0 ug/L 08/29/19 12:28 09/12/19 21 :49
Hexachloroethane ND H * 28 7.1 ug/L 08/29/19 12:28 09/12/19 21 :49
lndeno[1,2,3-cd]pyrene ND H 4.6 1.5 ug/L 08/29/19 12:28 09/12/19 21 :49
lsophorone ND H 9.3 0.62 ug/L 08/29/19 12:28 09/12/19 21 :49
N-Nitrosodi-n-propylamine ND H 9.3 0.52 ug/L 08/29/19 12:28 09/12/1921 :49
n-Nitrosodiphenylamine(as ND H 9.3 0.57 ug/L 08/29/19 12:28 09/12/19 21 :49
diphenylamine)
Naphthalene ND H* 3.7 0.37 ug/L 08/29/19 12:28 09/12/1921 :49
Nitrobenzene ND H 9.3 0.40 ug/L 08/29/19 12:28 09/12/19 21 :49
Pentachlorophenol ND H 46 5.1 ug/L 08/29/19 12:28 09/12/19 21 :49
Phenanthrene ND H 3.7 0.26 ug/L 08/29/19 12:28 09/12/1921 :49
Phenol ND H 9.3 0.52 ug/L 08/29/19 12:28 09/12/19 21 :49
Pyrene ND H 9.3 0.40 ug/L 08/29/19 12:28 09/12/19 21 :49
1,3-Dinitrobenzene ND H 9.3 0.90 ug/L 08/29/19 12:28 09/12/19 21 :49
1-Methylnaphthalene ND H * 3.7 0.33 ug/L 08/29/19 12:28 09/12/1921 :49
2,6-Dichlorophenol ND H 9.3 0.70 ug/L 08/29/19 12:28 09/12/19 21 :49
Aniline ND H 9.3 0.82 ug/L 08/29/19 12:28 09/12/19 21 :49
Azobenzene ND H 3.7 0.50 ug/L 08/29/19 12:28 09/12/1921 :49
Benzidine ND H 93 4.1 ug/L 08/29/19 12:28 09/12/19 21 :49
Benzyl alcohol ND H 9.3 0.33 ug/L 08/29/19 12:28 09/12/19 21 :49
Diphenylamine ND H 9.3 0.46 ug/L 08/29/19 12:28 09/12/19 21:49
N-Nitrosodimethylamine ND H 9.3 0.58 ug/L 08/29/19 12:28 09/12/19 21 :49
Pyridine ND H* 19 4.7 ug/L 08/29/19 12:28 09/12/19 21 :49
1,2-Diphenylhydrazine(as ND H 9.3 0.50 ug/L 08/29/19 12:28 09/12/1921 :49
Azobenzene)
3-Methylphenol ND H 9.3 0.37 ug/L 08/29/19 12:28 09/12/19 21 :49
4-Methylphenol ND H 9.3 0.95 ug/L 08/29/19 12:28 09/12/19 21 :49
Alachlor ND H 19 0.56 ug/L 08/29/19 12:28 09/12/19 21 :49
Famphur ND H 93 0.74 ug/L 08/29/19 12:28 09/12/19 21 :49
lndene ND H · 9.3 0.76 ug/L 08/29/19 12:28 09/12/19 21 :49
Total Cresols ND H 9.3 0.37 ug/L 08/29/19 12:28 09/12/1921 :49
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
2-Fluorophenol 41 17 -71 08/29119 12:28 09/12119 21:49 ---1
Phenol-d5 33 10-52 08129/19 12:28 09112119 21:49 1
2,4,6-Tribromophenol 65 52-123 08129/19 12:28 09/12119 21 :49 1
2-Fluorobiphenyl 56 47-119 08/29119 12:28 09/12119 21:49 1
Nitrobenzene-d5 73 45-113 08/29119 12:28 09/12119 21:49 1
Terphenyl-d14 31 X 50-123 08129/19 12:28 09112119 21:49 1
Eurofins TestAmerica, Denver
Page 20 of 54 Page 66 c9f2it/2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS)
Client Sample ID: C19081073-005D Lab Sample ID: 280-127755-14
Date Collected: 08/21/19 09:45 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
1, 1 '-Biphenyl ND H* 9.2 0.38 ug/L 08/29/19 12:28 09/12/19 22: 19 ---1
1,2,4,5-Tetrachlorobenzene ND H* 9.2 0.22 ug/L 08/29/19 12:28 09/12/19 22: 19 1
1,2,4-Trichlorobenzene ND H* 4.6 0.34 ug/L 08/29/19 12:28 09/12/19 22:19
1,2-Dichlorobenzene ND H* 4.6 0.28 ug/L 08/29/19 12:28 09/12/19 22: 19
1,3-Dichlorobenzene ND H* 9.2 1.8 ug/L 08/29/19 12:28 09/12/19 22:19
1,4-Dichlorobenzene ND H* 4.6 0.27 ug/L 08/29/19 12:28 09/12/19 22:19 I 1,4-Dioxane ND H 18 0.65 ug/L 08/29/19 12:28 09/12/19 22:19
2,4,6-Trichlorophenol ND H 9.2 0.68 ug/L 08/29/19 12:28 09/12/19 22:19
2,4-Dichlorophenol ND H 9.2 0.63 ug/L 08/29/19 12:28 09/12/19 22:19
2,2'-oxybis[1-chloropropane) ND H 9.2 0.39 ug/L 08/29/19 12:28 09/12/19 22:19
2,3,4,6-Tetrachlorophenol ND H 46 0.89 ug/L 08/29/19 12:28 09/12/19 22:19
2,4,5-Trichlorophenol ND H 9.2 0.48 ug/L 08/29/19 12:28 09/12/19 22: 19
2,4-Dimethylphenol ND H 9.2 0.62 ug/L 08/29/19 12:28 09/12/19 22:19
2,4-Dinitrotoluene ND H 9.2 0.86 ug/L 08/29/19 12:28 09/12/19 22: 19
2,6-Dinitrotoluene ND H 9.2 0.66 ug/L 08/29/19 12:28 09/12/19 22: 19
2-Chloronaphthalene ND H * 3.7 0.42 ug/L 08/29/19 12: 28 09/12/19 22: 19
2-Chlorophenol ND H 9.2 0.40 ug/L 08/29/19 12:28 09/12/19 22:19
2-Methylnaphthalene ND H* 3.7 0.38 ug/L 08/29/19 12:28 09/12/19 22:19
2-Methylphenol ND H 9.2 0.52 ug/L 08/29/19 12:28 09/12/19 22: 19
3 & 4 Methylphenol ND H 9.2 0.94 ug/L 08/29/19 12:28 09/12/19 22: 19
2-Nitroaniline ND H 9.2 0.83 ug/L 08/29/19 12:28 09/12/19 22: 19
2-Nitrophenol ND H 9.2 0.57 ug/L 08/29/19 12:28 09/12/19 22: 19
3,3'-Dichlorobenzidine ND H 46 0.77 ug/L 08/29/19 12:28 09/12/19 22:19
3-Nitroaniline ND H 9.2 0.72 ug/L 08/29/19 12:28 09/12/19 22:19
4,6-Dinitro-2-methylphenol ND H 46 5.4 ug/L 08/29/19 12:28 09/12/19 22:19 1
4-Bromophenyl phenyl ether ND H 9.2 0.38 ug/L 08/29/19 12:28 09/12/19 22:19 1
4-Chloro-3-methylphenol ND H 9.2 0.42 ug/L 08/29/19 12:28 09/12/19 22:19
4-Chloroaniline ND H 9.2 0.52 ug/L 08/29/19 12:28 09/12/19 22:19
4-Chlorophenyl phenyl ether ND H 9,2 0.58 ug/L 08/29/19 12:28 09/12/19 22:19
4-Nitroaniline ND H 9.2 0.77 ug/L 08/29/19 12:28 09/12/19 22 :19
4-Nitrophenol ND H 9.2 0.93 ug/L 08/29/19 12:28 09/12/19 22:19
Acenaphthene ND H 3.7 0.42 ug/L 08/29/19 12:28 09/12/19 22 :19
Acenaphthylene ND H* 3.7 0.46 ug/L 08/29/19 12:28 09/12/19 22 :19
Acetophenone ND H 9.2 0.48 ug/L 08/29/19 12:28 09/12/19 22 :19
Anthracene ND H 3.7 0.99 ug/L 08/29/19 12:28 09/12/19 22:19
Benzaldehyde ND H 9.2 0.49 ug/L 08/29/19 12:28 09/12/19 22:19
Benzo(a)pyrene ND H 3.7 0.59 ug/L 08/29/19 12:28 09/12/19 22:19 1
Benzo[b Jfluoranthene ND H 3.7 0.49 ug/L 08/29/19 12:28 09/12/19 22:19 1
Benzo[g ,h,i]perylene ND H 3.7 0.73 ug/L 08/29/19 12:28 09/12/19 22:19 1
Benzo(k]fluoranthene ND H 3.7 0.52 ug/L 08/29/19 12:28 09/12/19 22:19
Benzo[a]anthracene ND H 3.7 0.53 ug/L 08/29/19 12:28 09/12/19 22: 19
Bis(2-chloroethoxy)methane ND H 9.2 0.56 ug/L 08/29/19 12:28 09/12/19 22:19
Bis(2-chloroethyl)ether ND H 9.2 0.45 ug/L 08/29/19 12:28 09/12/19 22: 19
Bis(2-ethylhexyl) phthalate 1.1 JH 9.2 1.0 ug/L 08/29/19 12:28 09/12/19 22: 19
Butyl benzyl phthalate ND H 4.6 1.8 ug/L 08/29/19 12:28 09/12/19 22: 19
Caprolactam ND H 9.2 2.5 ug/L 08/29/19 12:28 09/12/19 22: 19
Carbazole ND H 3.7 1.2 ug/L 08/29/19 12:28 09/12/19 22: 19
Chrysene ND H 3.7 0.48 ug/L 08/29/19 12:28 09/12/19 22:19 1
Dibenz(a,h)anthracene ND H 3.7 0.60 ug/L 08/29/19 12:28 09/12/19 22: 19 1
Eurofins TestAmerica, Denver
Page 21 of 54 Page 67 c9@tl2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: C19081073-005D Lab Sample ID: 280-127755-14
Date Collected: 08/21/19 09:45 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Di-n-butyl phthalate ND ~ 3.7 0.81 ug/L -08/29/19 12:28 09/12/19 22: 19 --1
Di-n-octyl phthalate ND H 4.6 1.5 ug/L 08/29/19 12:28 09/12/19 22: 19
Dibenzofuran ND H 3.7 0.33 ug/L 08/29/19 12:28 09/12/19 22:19
Diethyl phthalate ND H 3.7 0.69 ug/L 08/29/19 12:28 09/12/19 22:19
Dimethyl phthalate ND H 3.7 1.2 ug/L 08/29/19 12:28 09/12/19 22:19
Fluoranthene ND H 3.7 0.59 ug/L 08/29/19 12:28 09/12/19 22:19 I Fluorene ND H 3.7 0.45 ug/L 08/29/19 12:28 09/12/19 22:19
Hexachlorobenzene ND H 9.2 0.89 ug/L 08/29/19 12:28 09/12/19 22:19
Hexachlorobutadiene ND H* 28 6.9 ug/L 08/29/19 12:28 09/12/19 22:19
Hexachloroethane ND H • 28 7.0 ug/L 08/29/19 12:28 09/12/19 22:19
lndeno[1,2,3-cd]pyrene ND H 4.6 1.5 ug/L 08/29/19 12:28 09/12/19 22: 19
lsophorone ND H 9.2 0.62 ug/L 08/29/19 12:28 09/12/19 22 :19
N-Nitrosodi-n-propylamine ND H 9.2 0.52 ug/L 08/29/19 12:28 09/12/19 22: 19
n-Nitrosodiphenylamine(as ND H 9.2 0.56 ug/L 08/29/19 12:28 09/12/19 22:19
diphenylamine)
Naphthalene ND H* 3.7 0.37 ug/L 08/29/19 12:28 09/12/19 22: 19
Nitrobenzene ND H 9.2 0.40 ug/L 08/29/19 12:28 09/12/19 22:19
Pentachlorophenol ND H 46 5.1 ug/L 08/29/19 12:28 09/12/19 22: 19
Phenanthrene ND H 3.7 0.26 ug/L 08/29/19 12:28 09/12/19 22:19
Phenol ND H 9.2 0.52 ug/L 08/29/19 12:28 09/12/19 22:19
Pyrene ND H 9.2 0.40 ug/L 08/29/19 12:28 09/12/19 22: 19
1,3-Dinitrobenzene ND H 9.2 0.89 ug/L 08/29/19 12:28 09/12/19 22:19
1-Methylnaphthalene ND H* 3.7 0.32 ug/L 08/29/19 12:28 09/12/19 22:19
2,6-Dichlorophenol ND H 9.2 0.69 ug/L 08/29/19 12:28 09/12/19 22:19
Aniline ND H 9.2 0.81 ug/L 08/29/19 12:28 09/12/19 22: 19
Azobenzene ND H 3.7 0.50 ug/L 08/29/19 12:28 09/12/19 22: 19
Benzidine ND H 92 4.1 ug/L 08/29/19 12:28 09/12/19 22:19
Benzyl alcohol ND H 9.2 0.32 ug/L 08/29/19 12:28 09/12/19 22:19
Diphenylamine ND H 9.2 0.45 ug/L 08/29/19 12:28 09/12/19 22: 19
Hexadecane ND H 9.2 0.33 ug/L 08/29/19 12:28 09/12119 22: 19
N-Nitrosodimethylamine ND H 9.2 0.57 ug/L 08/29/19 12:28 09/12119 22:19
Pyridine ND H* 18 4.6 ug/L 08/29/19 12:28 09112/19 22:19
1,2-Diphenylhydrazine(as ND H 9.2 0.50 ug/L 08/29/19 12:28 09/12/19 22:19
Azobenzene)
3-Methylphenol ND H 9.2 0.37 ug/L 08/29119 12:28 09112119 22:19
4-Methylphenol ND H 9.2 0.94 ug/L 08/29/19 12:28 09/12119 22:19
Alachlor ND H 18 0.55 ug/L 08/29/19 12:28 09112/19 22:19
Famphur ND H 92 0.73 ug/L 08/29/19 12:28 09/12119 22: 19
lndene ND H * 9.2 0.76 ug/L 08/29/19 12:28 09112119 22: 19
Total Cresols ND H 9.2 0.37 ug/L 08/29/1912:28 09112119 22:19
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fae
2-Fluoropheno/ 48 17-71 08/29/19 12:28 09/12119 22:19 --1
Phenol-d5 37 10-52 08/29/19 12:28 09/12119 22:19 1
2,4, 6-Tribromophenol 79 52-123 08129/19 12:28 09/12119 22:19 1
2-Fluorobiphenyl 67 47-119 08/29/19 12:28 09/12119 22:19 1
Nitrobenzene-d5 77 45-113 08/29/19 12:28 09/12119 22:19 1
Terphenyl-d14 57 50-123 08/29/19 12:28 09/12119 22:19 1
Eurofins TestAmerica, Denver
Page 22 of 54 Page 68 c9~2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
ProjecUSite: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS)
Client Sample ID: C19081073-006D Lab Sample ID: 280-127755-17
Date Collected: 08/21/19 10:15 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
1, 1 '-Biphenyl ND H* 8.8 0.36 ug/L 08/29/19 12:28 09/12/19 22:48 ---1
1,2,4,5-Tetrachlorobenzene ND H* 8.8 0.21 ug/L 08/29/19 12:28 09/12/19 22:48
1,2,4-Trichlorobenzene ND H* 4.4 0.32 ug/L 08/29/19 12:28 09/12/19 22:48
1,2-Dichlorobenzene ND H* 4.4 0.27 ug/L 08/29/19 12:28 09/12/19 22:48
1,3-Dichlorobenzene ND H* 8.8 1.8 ug/L 08/29/19 12:28 09/12/19 22:48
1,4-Dichlorobenzene ND H* 4.4 0.26 ug/L 08/29/19 12:28 09/12/19 22:48 I 1,4-Dioxane ND H 18 0.62 ug/L 08/29/19 12:28 09/12/19 22:48
2,4,6-Trichlorophenol ND H 8.8 0.65 ug/L 08/29/19 12:28 09/12/19 22:48
2,4-Dichlorophenol ND H 8.8 0.60 ug/L 08/29/19 12:28 09/12/19 22:48
2,2'-oxybis[1-chloropropane] ND H 8.8 0.37 ug/L 08/29/19 12:28 09/12/19 22:48
2,3,4,6-Tetrachlorophenol ND H 44 0.84 ug/L 08/29/19 12:28 09/12/19 22:48
2,4,5-Trichlorophenol ND H 8.8 0.46 ug/L 08/29/19 12:28 09/12/19 22:48
2 ,4-Dimethylphenol ND H 8.8 0.59 ug/L 08/29/19 12:28 09/12/19 22:48
2,4-Dinitrotoluene ND H 8.8 0.81 ug/L 08/29/19 12:28 09/12/19 22:48
2,6-Dinitrotoluene ND H 8.8 0.63 ug/L 08/29/19 12:28 09/12/19 22:48
2-Chloronaphthalene ND H* 3.5 0.40 ug/L 08/29/19 12:28 09/12/19 22:48
2-Chlorophenol ND H 8.8 0.38 ug/L 08/29/19 12:28 09/12/19 22:48
2-Methylnaphthalene ND H* 3.5 0.36 ug/L 08/29/19 12:28 09112119 22:48
2-Methylphenol ND H 8.8 0.49 ug/L 08129/19 12:28 09/12/19 22:48
3 & 4 Methylphenol ND H 8.8 0.89 ug/L 08/29/19 12:28 09/12/19 22:48
2-Nitroaniline ND H 8.8 0.79 ug/L 08/29/19 12:28 09/12/19 22:48
2-Nitrophenol ND H 8.8 0.54 ug/L 08/29/19 12:28 09/12/19 22:48
3,3'-Dichlorobenzidine ND H 44 0.73 ug/L 08/29/19 12:28 09/12/19 22:48
3-Nitroaniline ND H 8.8 0.68 ug/L 08/29/19 12:28 09/12/19 22:48
4,6-Dinitro-2-methylphenol ND H 44 5.1 ug/L 08/29/19 12:28 09/12/19 22:48
4-Bromophenyl phenyl ether ND H 8.8 0.36 ug/L 08/29/19 12:28 09/12/19 22:48
4-Chloro-3-methylphenol ND H 8.8 0.39 ug/L 08/29/19 12:28 09/12/19 22:48
4-Chloroaniline ND H 8.8 0.49 ug/L 08/29/19 12:28 09/12/19 22:48
4-Chlorophenyl phenyl ether ND H 8.8 0.55 ug/L 08/29/19 12:28 09/12/19 22:48
4-Nitroaniline ND H 8.8 0.74 ug/L 08/29/19 12:28 09/12/19 22:48
4-Nitrophenol ND H 8.8 0.88 ug/L 08/29/19 12:28 09/12/19 22:48
Acenaphthene ND H 3.5 0.39 ug/L 08/29/19 12:28 09/12/19 22:48
Acenaphthylene ND H* 3.5 0.44 ug/L 08/29/19 12:28 09/12/19 22:48
Acetophenone ND H 8.8 0.46 ug/L 08/29/19 12:28 09/12/19 22:48
Anthracene 1.7 JH 3.5 0.94 ug/L 08/29/19 12:28 09/12/19 22:48
Benzaldehyde ND H 8.8 0.46 ug/L 08/29/19 12:28 09/12/19 22:48
Benzo[a]pyrene ND H 3.5 0.56 ug/L 08/29/19 12:28 09/12/19 22:48
Benzo[b]fluoranthene ND H 3.5 0.46 ug/L 08/29/19 12:28 09/12/19 22:48
Benzo[g, h ,i]perylene ND H 3.5 0.69 ug/L 08/29/19 12:28 09/12/19 22:48
Benzo[k]fluoranthene ND H 3.5 0.49 ug/L 08/29/19 12:28 09/12/19 22:48
Benzo[ a ]anthracene ND H 3.5 0.51 ug/L 08/29/19 12:28 09/12/19 22:48
Bis(2-chloroethoxy)methane ND H 8.8 0.53 ug/L 08/29/19 12:28 09/12/19 22:48
Bis(2-chloroethyl)ether ND H 8.8 0.43 ug/L 08/29/19 12:28 09/12/19 22:48
Bis(2-ethylhexyl) phthalate ND H 8.8 0.98 ug/L 08/29/19 12:28 09/12/19 22:48
Butyl benzyl phthalate ND H 4.4 1.8 ug/L 08/29/19 12:28 09/12/19 22:48
Caprolactam ND H 8.8 2.4 ug/L 08/29/19 12:28 09/12/19 22:48
Carbazole ND H 3.5 1.2 ug/L 08/29/19 12:28 09/12/19 22:48
Chrysene ND H 3.5 0.46 ug/L 08/29/19 12:28 09/12/19 22:48
Dibenz(a,h)anthracene ND H 3.5 0.57 ug/L 08/29/19 12:28 09/12/19 22:48
Eurofins TestAmerica, Denver
Page 23 of 54 Page 69 c9/M/2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: C19081073-006D Lab Sample ID: 280-127755-17
Date Collected: 08/21/1910:15 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Di-n-butyl phthalate -------ND H --~ 0.77 ug/L 08/29/19 12:28 09/12/19 22:48 ---1
Di-n-octyl phthalate ND H 4.4 1.4 ug/L 08/29/19 12:28 09/12/19 22:48
Dibenzofuran ND H 3.5 0.32 ug/L 08/29/19 12:28 09/12/19 22:48
Diethyl phthalate ND H 3.5 0.66 ug/L 08/29/19 12:28 09/12/19 22:48
Dimethyl phthalate ND H 3.5 1.1 ug/L 08/29/19 12:28 09/12/19 22:48
Fluoranthene ND H 3.5 0.56 ug/L 08/29/19 12:28 09/12/19 22:48 I Fluorene ND H 3.5 0.43 ug/L 08/29/19 12:28 09/12/19 22:48
Hexachlorobenzene ND H 8.8 0.84 ug/L 08/29/19 12:28 09/12/19 22:48
Hexachlorobutadiene ND H · 26 6.6 ug/L 08/29/19 12:28 09/12/19 22:48
Hexachloroethane ND H · 26 6.7 ug/L 08/29/19 12:28 09/12/19 22:48
lndeno[1,2,3-cd]pyrene ND H 4.4 1.4 ug/L 08/29/19 12:28 09/12/19 22:48
lsophorone ND H 8.8 0.59 ug/L 08/29/19 12:28 09/12/19 22:48
N-Nitrosodi-n-propylamine ND H 8.8 0.49 ug/L 08/29/19 12:28 09/12/19 22:48
n-Nitrosodiphenylamine(as ND H 8.8 0.53 ug/L 08/29/19 12:28 09/12/19 22:48
diphenylamine)
Naphthalene ND H" 3.5 0.35 ug/L 08/29/19 12:28 09/12/19 22:48
Nitrobenzene ND H 8.8 0.38 ug/L 08/29/19 12:28 09/12/19 22:48
Pentachlorophenol ND H 44 4.8 ug/L 08/29/19 12:28 09/12/19 22:48
Phenanthrene ND H 3.5 0.25 ug/L 08/29/19 12:28 09/12/19 22:48
Phenol ND H 8.8 0.49 ug/L 08/29/19 12:28 09/12/19 22:48
Pyrene ND H 8.8 0.38 ug/L 08/29/19 12:28 09/12/19 22:48
1,3-Dinitrobenzene ND H 8.8 0.85 ug/L 08/29/19 12:28 09/12/19 22:48
1-Methylnaphthalene ND H" 3.5 0.31 ug/L 08/29/19 12:28 09/12/19 22:48
2,6-Dichlorophenol ND H 8.8 0.66 ug/L 08/29/19 12:28 09/12/19 22:48
Aniline ND H 8.8 0.77 ug/L 08/29/19 12:28 09/12/19 22:48
Azobenzene ND H 3.5 0.47 ug/L 08/29/1912:28 09/12/19 22:48
Benzidine ND H 88 3.9 ug/L 08/29/19 12:28 09/12/19 22:48
Benzyl alcohol ND H 8.8 0.31 ug/L 08/29/19 12:28 09/12/19 22:48
Diphenylamine ND H 8.8 0.43 ug/L 08/29/19 12:28 09/12/19 22:48
N-Nitrosodimethylamine ND H 8.8 0.54 ug/L 08/29/19 12:28 09/12/19 22:48
Pyridine ND H* 18 4.4 ug/L 08/29/19 12:28 09/12/19 22:48
1,2-Diphenylhydrazine(as ND H 8.8 0.47 ug/L 08/29/19 12:28 09/12/19 22:48
Azobenzene)
3-Methylphenol ND H 8.8 0.35 ug/L 08/29/19 12:28 09/12/19 22:48
4-Methylphenol ND H 8.8 0.89 ug/L 08/29/19 12:28 09/12/19 22:48
Alachlor ND H 18 0.53 ug/L 08/29/19 12:28 09/12/19 22:48 1
Famphur ND H 88 0.70 ug/L 08/29/19 12:28 09/12/19 22:48 1
lndene ND H* 8.8 0.72 ug/L 08/29/19 12:28 09/12/19 22:48 1
Total Cresols ND H 8.8 0.35 ug/L 08/29/19 12:28 09/12/19 22:48
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
2-Fluoropheno/ 48 17 -71 08129/19 12:28 09/12119 22:48 ---1
Phenol-d5 42 10-52 08/29119 12:28 09/12/19 22:48
2,4, 6-Tribromophenol 58 52-123 08/29119 12:28 09112119 22.48 1
2-Fluorobiphenyl 41 X 47 -119 08/29119 12:28 09/12/19 22:48 1
Nitrobenzene-d5 62 45-113 08129/19 12:28 09/12/19 22:48 1
Terphenyl-d14 31 X 50-123 08/29119 12:28 09/12119 22:48 1
Eurofins TestAmerica, Denver
Page 24 of 54 Page 70 dJIM/2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS)
Client Sample ID: C19081073-007D Lab Sample ID: 280-127755-20
Date Collected: 08/21/19 10:30 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
1, 1 '-Biphenyl ND H • 9.1 0.37 ug/L 08/29/19 12:28 09/12/19 23: 17 ---1
1,2 ,4,5-Tetrachlorobenzene ND H* 9.1 0.22 ug/L 08/29/19 12:28 09/12/19 23: 17
1,2 ,4-Trichlorobenzene ND H* 4.5 0.33 ug/L 08/29/19 12:28 09/12/19 23: 17
1,2-Dichlorobenzene ND H* 4.5 0.28 ug/L 08/29/19 12:28 09/12/19 23: 17
1,3-Dichlorobenzene ND H* 9.1 1.8 ug/L 08/29/19 12:28 09/12/19 23: 17
1,4-Dichlorobenzene ND H* 4.5 0.27 ug/L 08/29/19 12:28 09/12/19 23:17 I 1,4-Dioxa ne ND H 18 0.65 ug/L 08/29/19 12:28 09/12/19 23: 17
2,4,6-Trichlorophenol ND H 9.1 0.67 ug/L 08/29/19 12:28 09/12/19 23:17
2,4-Dichlorophenol ND H 9.1 0.62 ug/L 08/29/19 12:28 09/12/19 23:17
2,2'-oxybis[1-chloropropane] ND H 9.1 0.38 ug/L 08/29/19 12:28 09/12/19 23:17
2,3,4,6-Tetrachlorophenol ND H 45 0.87 ug/L 08/29/1-9 12:28 09/12/19 23:17
2,4,5-Trichlorophenol ND H 9.1 0.47 ug/L 08/29/19 12:28 09/12/19 23: 17
2,4-Dimethylphenol ND H 9.1 0.61 ug/L 08/29/19 12:28 09/12/19 23: 17
2,4-Dinitrotoluene ND H 9.1 0.84 ug/L 08/29/19 12:28 09/12/19 23:17
2,6-Dinitrotoluene ND H 9.1 0.65 ug/L 08/29/19 12:28 09/12/19 23:17
2-Chloronaphthalene ND H* 3.6 0.42 ug/L 08/29/19 12:28 09/12/19 23:17
2-Chlorophenol ND H 9.1 0.39 ug/L 08/29/19 12:28 09/12/19 23:17
2-Methylnaphthalene ND H* 3.6 0.37 ug/L 08/29/19 12:28 09/12/19 23:17
2-Methylphenol ND H 9.1 0.51 ug/L 08/29/19 12:28 09/12/19 23:17
3 & 4 Methylphenol ND H 9.1 0.93 ug/L 08/29/19 12:28 09/12/19 23:17
2-Nitroaniline ND H 9.1 0.82 ug/L 08/29/19 12:28 09/12/19 23: 17
2-Nitrophenol ND H 9.1 0.56 ug/L 08/29/19 12:28 09/12/19 23:17
3,3'-Dichlorobenzidine ND H 45 0.75 ug/L 08/29/19 12:28 09/12/19 23:17
3-Nitroaniline ND H 9.1 0.71 ug/L 08/29/19 12:28 09/12/19 23:17
4,6-Dinitro-2-methylphenol ND H 45 5.3 ug/L 08/29/19 12:28 09/12/19 23:17
4-Bromophenyl phenyl ether ND H 9.1 0.37 ug/L 08/29/19 12:28 09/12/19 23:17
4-Chloro-3-methylphenol ND H 9.1 0.41 ug/L 08/29/19 12:28 09/12/1923: 17
4-Chloroaniline ND H 9.1 0.51 ug/L 08/29/19 12:28 09/12/19 23: 17
4-Chlorophenyl phenyl ether ND H 9.1 0.57 ug/L 08/29/19 12:28 09/12/19 23: 17
4-Nitroaniline ND H 9.1 0.76 ug/L 08/29/19 12:28 09/12/19 23: 17
4-Nitrophenol ND H 9.1 0.92 ug/L 08/29/19 12:28 09/12/19 23: 17
Acenaphthene ND H 3.6 0.41 ug/L 08/29/19 12:28 09/12/19 23: 11
Acenaphthylene ND H* 3.6 0.45 ug/L 08/29/19 12:28 09/12/19 23: 17
Acetophenone ND H 9.1 0.47 ug/L 08/29/19 12:28 09/12/19 23: 17
Anthracene ND H 3.6 0.97 ug/L 08/29/19 12:28 09/12/19 23: 17
Benzaldehyde ND H 9.1 0.48 ug/L 08/29/19 12:28 09/12/19 23:17
Benzo[a]pyrene ND H 3.6 0.58 ug/L 08/29/19 12:28 09/12/19 23:17
Benzo[b]fluoranthene ND H 3.6 0.48 ug/L 08/29/19 12:28 09/12/19 23:17
Benzo[g ,h,i]perylene ND H 3.6 0.72 ug/L 08/29/19 12:28 09/12/19 23: 17
Benzo[k]fluoranthene ND H 3.6 0.51 ug/L 08/29/19 12:28 09/12/19 23: 17
Benzo[a]anthracene ND H 3.6 0.53 ug/L 08/29/19 12:28 09/12/19 23: 17
Bis(2-chloroethoxy)methane ND H 9.1 0.55 ug/L 08/29/19 12:28 09/12/19 23: 17
Bis(2-chloroethyl)ether ND H 9.1 0.45 ug/L 08/29/19 12:28 09/12/19 23:17
Bis(2-ethylhexyl) phthalate 16 H 9.1 1.0 ug/L 08/29/19 12:28 09/12/19 23:17
Butyl benzyl phthalate ND H 4.5 1.8 ug/L 08/29/19 12:28 09/12/19 23:17
Caprolactam ND H 9.1 2.5 ug/L 08/29/19 12:28 09/12/19 23:17
Carbazole ND H 3.6 1.2 ug/L 08/29/19 12:28 09/12/19 23:17
Chrysene ND H 3.6 0.47 ug/L 08/29/19 12:28 09/12/19 23:17
Dibenz(a,h)anthracene ND H 3.6 0.59 ug/L 08/29/19 12:28 09/12/19 23:17
Eurofins TestAmerica, Denver
Page 25 of 54 Page 71 <9/2412019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: C19081073-007D Lab Sample ID: 280-127755-20
Date Collected: 08/21 /19 10: 30 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Di-n-butyl phthalate ND H 3.6 ~ ug/L 08/29/19 12:28 09/12/19 23: 17 --1
Di-n-octyl phthalate ND H 4.5 1.4 ug/L 08/29/19 12:28 09/12/19 23: 17
Dibenzofuran ND H 3.6 0.33 ug/L 08/29/19 12 :28 09/12/19 23:17
Diethyl phthalate ND H 3.6 0.68 ug/L 08/29/19 12:28 09/12/19 23:17
Dimethyl phthalate ND H 3.6 1.1 ug/L 08/29/19 12:28 09/12/19 23:17
Fluoranthene ND H 3.6 0.58 ug/L 08/29/19 12:28 09/12/19 23:17 1 I Fluorene ND H 3.6 0.45 ug/L 08/29/19 12:28 09/12/19 23:17 1
Hexachlorobenzene ND H 9.1 0.87 ug/L 08/29/19 12:28 09/12/19 23:17
Hexachlorobutadiene ND H* 27 6.8 ug/L 08/29/19 12:28 09/12/19 23: 17
Hexachloroethane ND H* 27 6.9 ug/L 08/29/19 12:28 09/12/19 23: 17
lndeno[1,2,3-cd]pyrene ND H 4.5 1.5 ug/L 08/29/19 12:28 09/12/19 23: 17
lsophorone ND H 9.1 0.61 ug/L 08/29/19 12 :28 09/12/1923: 17
N-Nitrosodi-n-propylamine ND H 9.1 0.51 ug/L 08/29/19 12:28 09/12/19 23:17
n-Nitrosodiphenylamine(as ND H 9.1 0.55 ug/L 08/29/19 12:28 09/12/19 23:17
diphenylamine)
Naphthalene ND H • 3.6 0.36 ug/L 08/29/19 12:28 09/12/19 23:17
Nitrobenzene ND H 9.1 0.39 ug/L 08/29/19 12:28 09/12/19 23: 17
Pentachlorophenol ND H 45 5.0 ug/L 08/29/19 12:28 09/12/19 23: 17
Phenanthrene ND H 3.6 0.25 ug/L 08/29/19 12:28 09/12/19 23: 17
Phenol ND H 9.1 0.51 ug/L 08/29/19 12:28 09/12/19 23: 17 1
Pyrene ND H 9.1 0.39 ug/L 08/29/19 12:28 09/12/19 23:17 1
1,3-Dinitrobenzene ND H 9.1 0.88 ug/L 08/29/19 12:28 09/12/19 23:17
1-Methylnaphthalene ND w 3.6 0.32 ug/L 08/29/19 12:28 09/12/19 23:17
2,6-Dichlorophenol ND H 9.1 0.68 ug/L 08/29/19 12:28 09/12/19 23:17
Aniline ND H 9.1 0.80 ug/L 08/29/19 12:28 09/12/19 23:17
Azobenzene ND H 3.6 0.49 ug/L 08/29/19 12:28 09/12/19 23: 17
Benzidine ND H 91 4.0 ug/L 08/29/19 12:28 09/12/19 23: 17
Benzyl alcohol ND H 9.1 0.32 ug/L 08/29/19 12:28 09/12/19 23: 17
Diphenylamine ND H 9.1 0.45 ug/L 08/29/19 12:28 09/12/19 23:17
Hexadecane ND H 9.1 0.32 ug/L 08/29/19 12:28 09/12/19 23:17
N-Nitrosodimethylamine ND H 9.1 0.56 ug/L 08/29/19 12:28 09/12/19 23:17
Pyridine ND H • 18 4.6 ug/L 08/29/19 12:28 09/12/19 23: 17
1,2-Diphenylhydrazine(as ND H 9.1 0.49 ug/L 08/29/19 12:28 09/12/19 23: 17
Azobenzene)
3-Methylphenol 0.42 JH 9.1 0.36 ug/L 08/29/19 12 :28 09/12/19 23:17
4-Methylphenol ND H 9.1 0.93 ug/L 08/29/19 12:28 09/12/19 23:17 1
Alachlor ND H 18 0.55 ug/L 08/29/19 12:28 09/12/19 23:17 1
Famphur ND H 91 0.72 ug/L 08/29/19 12:28 09/12/19 23:17
lndene ND H* 9.1 0.74 ug/L 08/29/19 12:28 09/12/19 23:17
Total Cresols 0.42 JH 9.1 0.36 ug/L 08/29/19 12:28 09/12/19 23: 17
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
2-Fluorophenol 50 17-71 08/29/19 12:28 09/12119 23:17 1
Phenol-d5 40 10-52 08129/19 12:28 09/12119 23:17 1
2, 4, 6-Tribromophenol 68 52-123 08/29119 12:28 09/12119 23:17 1
2-Fluorobiphenyl 59 47-119 08/29/19 12:28 09/12119 23:17
Nitrobenzene-d5 67 45_ 113 08129/19 12:28 09/12119 23:17
Terphenyl-d14 59 50-123 08/29119 12:28 09/12119 23:17 1
Eurofins TestAmerica, Denver
Page 26 of 54 Page 72 c9@t!2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS)
Client Sample ID: C19081073-008D Lab Sample ID: 280-127755-23
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
1, 1 '-Biphenyl ND Fl-9.9 0.40 ug/L 08/29/19 12:28 09/12/19 23:47 1
1,2,4,5-Tetrachlorobenzene ND H* 9.9 0.24 ug/L 08/29/19 12:28 09/12/19 23:47 1
1,2,4-Trichlorobenzene ND H* 4.9 0.36 ug/L 08/29/19 12:28 09/12/19 23:47
1,2-Dichlorobenzene ND H* 4.9 0.30 ug/L 08/29/19 12:28 09/12/19 23:4 7
1,3-Dichlorobenzene ND H* 9.9 2.0 ug/L 08/29/19 12:28 09/12/19 23:4 7
1 ,4-Dichlorobenzene ND H* 4.9 0.29 ug/L 08/29/19 12:28 09/12/19 23:47 I 1,4-Dioxane ND H 20 0.70 ug/L 08/29/19 12:28 09/12/19 23:47
2,4,6-Trichlorophenol 5.2 JH 9.9 0.73 ug/L 08/29/19 12:28 09/12/19 23:47
2,4-Dichlorophenol ND H 9.9 0.67 ug/L 08/29/19 12:28 09/12/19 23:47
2,2'-oxybis[1-chloropropane] ND H 9.9 0.41 ug/L 08/29/19 12:28 09/12/19 23:47
2,3,4,6-Tetrachlorophenol ND H 49 0.95 ug/L 08/29/19 12:28 09/12/19 23:47
2,4,5-Trichlorophenol ND H 9.9 0.51 ug/L 08/29/19 12:28 09/12/19 23:47
2,4-Dimethylphenol ND H 9.9 0.66 ug/L 08/29/19 12:28 09/12/19 23:4 7
2,4-Dinitrotoluene ND H 9.9 0.92 ug/L 08/29/19 12:28 09/12/19 23:47
2,6-Dinitrotoluene ND H 9.9 0.71 ug/L 08/29/19 12:28 09/12/19 23:4 7
2-Chloronaphthalene ND H* 3.9 0.45 ug/L 08/29/19 12:28 09/12/19 23:47
2-Chlorophenol ND H 9.9 0.42 ug/L 08/29/19 12:28 09/12/19 23:4 7
2-Methylnaphthalene ND H* 3.9 0.40 ug/L 08/29/19 12:28 09/12/19 23:47
2-Methylphenol ND H 9.9 0.55 ug/L 08/29/19 12:28 09/12/19 23:47
3 & 4 Methylphenol ND H 9.9 1.0 ug/L 08/29/19 12:28 09/12/19 23:47
2-Nitroaniline ND H 9.9 0.89 ug/L 08/29/19 12:28 09/12/19 23:47
2-Nitrophenol ND H 9.9 0.61 ug/L 08/29/19 12:28 09/12/19 23:47
3,3'-Dichlorobenzidine ND H 49 0.82 ug/L 08/29/19 12:28 09/12/19 23:4 7
3-Nitroaniline ND H 9.9 0.77 ug/L 08/29/19 12:28 09/12/19 23:4 7 1
4,6-Dinitro-2-methylphenol ND H 49 5.8 ug/L 08/29/19 12:28 09/12/19 23:47 1
4-Bromophenyl phenyl ether ND H 9.9 0.40 ug/L 08/29/19 12:28 09/12/19 23:47 1
4-Chloro-3-methylphenol ND H 9.9 0.44 ug/L 08/29/19 12:28 09/12/19 23:4 7 1
4-Chloroaniline ND H 9.9 0.55 ug/L 08/29/19 12:28 09/12/19 23:47
4-Chlorophenyl phenyl ether ND H 9.9 0.62 ug/L 08/29/19 12:28 09/12/19 23:47
4-Nitroaniline ND H 9.9 0.83 ug/L 08/29/19 12:28 09/12/19 23:47
4-Nitrophenol ND H 9.9 1.0 ug/L 08/29/19 12:28 09/12/19 23:4 7
Acenaphthene ND H 3.9 0.44 ug/L 08/29/19 12:28 09/12/19 23:4 7
Acenaphthylene ND H* 3.9 0.49 ug/L 08/29/19 12:28 09/12/19 23:47
Acetophenone ND H 9.9 0.51 ug/L 08/29/19 12:28 09/12/19 23:4 7
Anthracene ND H 3.9 1.1 ug/L 08/29/19 12:28 09/12/19 23:47
Benzaldehyde ND H 9.9 0.52 ug/L 08/29/19 12:28 09/12/19 23:47
Benzo[a)pyrene ND H 3.9 0.63 ug/L 08/29/19 12:28 09/12/19 23:47
Benzo[b]fluoranthene ND H 3.9 0.52 ug/L 08/29/19 12:28 09/12/19 23:47
Benzo[g,h,i]perylene ND H 3.9 0.78 ug/L 08/29/19 12:28 09/12/19 23:4 7
Benzo[k]fluoranthene ND H 3.9 0.55 ug/L 08/29/19 12:28 09/12/19 23:4 7
Benzo[a]anthracene ND H 3.9 0.57 ug/L 08/29/19 12:28 09/12/19 23:4 7
Bis(2-chloroethoxy)methane ND H 9.9 0.60 ug/L 08/29/19 12:28 09/12/19 23:4 7
Bis(2-chloroethyl)ether ND H 9.9 0.48 ug/L 08/29/19 12:28 09/12/19 23:47
Bis(2-ethylhexyl) phthalate ND H 9.9 1.1 ug/L 08/29/19 12:28 09/12/19 23:47 1
Butyl benzyl phthalate ND H 4.9 2.0 ug/L 08/29/19 12:28 09/12/19 23:47 1
Caprolactam ND H 9.9 2.7 ug/L 08/29/19 12 28 09/12/19 23:4 7 1
Carbazole ND H 3.9 1.3 ug/L 08/29/19 12:28 09/12/19 23:47 1
Chrysene ND H 3.9 0.51 ug/L 08/29/19 12:28 09/12/19 23:4 7 1
Dibenz(a,h)anthracene ND H 3.9 0.64 ug/L 08/29/19 12:28 09/12/19 23:4 7
Eurofins TestAmerica, Denver
Page 27 of 54 Page 73 c910t'2019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
ProjecVSite: 11 (e} Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: C19081073-008D Lab Sample ID: 280-127755-23
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
Di-n-butyl phthalate ND H 3.9 0.87 ug/L 08/29/19 12:28 09/12/19 23:4 7 --1
Di-n-octyl phthalate ND H 4.9 1.6 ug/L 08/29/19 12:28 09/12/19 23:47
Dibenzofuran ND H 3.9 0.36 ug/L 08/29/19 12:28 09/12/19 23:4 7
Diethyl phthalate ND H 3.9 0.74 ug/L 08/29/19 12:28 09/12/19 23:4 7
Dimethyl phthalate ND H 3.9 1.2 ug/L 08/29/19 12:28 09/12/19 23:47
Fluoranthene ND H 3.9 0.63 ug/L 08/29/19 12:28 09/12/19 23:47 I Fluorene ND H 3.9 0.48 ug/L 08/29/19 12:28 09/12/19 23:47
Hexachlorobenzene ND H 9.9 0.95 ug/L 08/29/19 12:28 09/12/19 23:4 7
Hexachlorobutadiene ND H * 30 7.4 ug/L 08/29/19 12:28 09/12/19 23:47
Hexachloroethane ND H* 30 7.5 ug/L 08/29/19 12:28 09/12/19 23:47
lndeno[1 ,2,3-cd]pyrene ND H 4.9 1.6 ug/L 08/29/19 12:28 09/12/19 23:4 7
lsophorone ND H 9.9 0.66 ug/L 08/29/1912:28 09/12/19 23:47
N-Nitrosodi-n-propylamine ND H 9.9 0.55 ug/L 08/29/19 12:28 09/12/19 23:47
n-Nitrosodiphenylamine(as ND H 9.9 0.60 ug/L 08/29/19 12:28 09/12/19 23:4 7
diphenylamine)
Naphthalene ND H * 3.9 0.39 ug/L 08/29/19 12 :28 09/12/19 23:47
Nitrobenzene ND H 9.9 0.42 ug/L 08/29/19 12:28 09/12/19 23:4 7
Pentachlorophenol ND H 49 5.4 ug/L 08/29/19 12:28 09/12/19 23:4 7
Phenanthrene ND H 3.9 0.28 ug/L 08/29/19 12:28 09/12/19 23:47
Phenol ND H 9.9 0.55 ug/L 08/29/19 12:28 09/12/19 23:47
Pyrene ND H 9.9 0.42 ug/L 08/29/19 12:28 09/12/19 23:4 7
1,3-Dinitrobenzene ND H 9.9 0.96 ug/L 08/29/19 12:28 09/12/19 23:4 7 1
1-Methylnaphthalene ND H • 3.9 0.35 ug/L 08/29/19 12:28 09/12/19 23:47 1
2,6-Dichlorophenol ND H 9.9 0.74 ug/L 08/29/19 12:28 09/12/19 23:4 7
Aniline ND H 9.9 0.87 ug/L 08/29/19 12:28 09/12/19 23:4 7
Azobenzene ND H 3.9 0.53 ug/L 08/29/19 12:28 09/12/19 23:47
Benzidine ND H 99 4.3 ug/L 08/29/19 12:28 09/12/19 23:4 7
Benzyl alcohol ND H 9.9 0.35 ug/L 08/29/19 12:28 09/12/19 23:4 7
Diphenylamine ND H 9.9 0.48 ug/L 08/29/19 12:28 09/12/19 23:47
Hexadecane 91 H 9.9 0.35 ug/L 08/29/19 12:28 09/12/19 23:47
N-Nitrosodimethylamine ND H 9.9 0.61 ug/L 08/29/19 12:28 09/12/19 23:4 7
Pyridine ND H • 20 5.0 ug/L 08/29/19 12:28 09/12/19 23:47
1,2-Diphenylhydrazine(as ND H 9.9 0.53 ug/L 08/29/19 12:28 09/12/19 23:47 1
Azobenzene)
3-Methylphenol ND H 9.9 0.39 ug/L 08/29/19 12:28 09/12/19 23:47
4-Methylphenol ND H 9.9 1.0 ug/L 08/29/19 12:28 09/12/19 23:47
Alachlor ND H 20 0.59 ug/L 08/29/19 12:28 09/12/19 23:47
Famphur ND H 99 0.78 ug/L 08/29/19 12:28 09/12/19 23:47
lndene ND H • 9.9 0.81 ug/L 08/29/19 12:28 09/12/19 23:47
Total Cresols ND H 9.9 0.39 ug/L 08/29/19 12:28 09/12/19 23:47
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
2-Fluorophenol 40 17 -71 08/29/19 12:28 09/12/19 23:47 --1
Phenol-d5 37 10-52 08/29119 12:28 09112/19 23:47 1
2,4, 6-Tribromophenol 46 X 52-123 08129/19 12:28 09/12119 23:47 1
2-Fluorobiphenyl 32 X 47 -119 08129/19 12:28 09/12119 23:47 1
Nitrobenzene-d5 50 45 _ 113 08/29/19 12:28 09/12119 23:47 1
Terphenyl-d14 32 X 50-123 08/29119 12:28 09112/19 23:47 1
Eurofins TestAmerica, Denver
Page 28 of 54 Page 74 <9/2412019
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) -DL
Client Sample ID: C19081073-004D Lab Sample ID: 280-127755-11
Date Collected: 08/21/19 09:40 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Hexadecane 320 H 37 1.3 ug/L 08/29/19 12:28 09/17 /19 15:48 ---4
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
2-Fluorophenol 43 D 17 -71 08/29/19 12:28 09117/19 15:48 --4
Phenol-d5 33 D 10-52 08/29/19 12:28 09117/19 15:48 4
2,4, 6-Tribromophenol 61 D 52-123 08/29/19 12:28 09/17/19 15:48 4 I 2-Fluorobiphenyl 59 D 47 -119 08129/19 12:28 09117/19 15:48 4
Nitrobenzene-d5 71 D 45-113 08/29/19 12:28 09117/19 15:48 4
Terphenyl-d14 34 DX 50-123 08/29/19 12:28 09117/19 15:48 4
Client Sample ID: C19081073-006D Lab Sample ID: 280-127755-17
Date Collected: 08/21/19 10: 15 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Hexadecane 190 H --~ 1.2 ug/L -08/29/19 12:28 09/17/1916:18 --4
Surrogate %Recovery Qualifier Limits Prepared Analyzed Di/ Fae
2-Fluorophenol 51 D 17 -71 08/29/19 12:28 09117/19 16:18 --4
Phenol-d5 45 D 10-52 08129/19 12:28 09117/19 16:18 4
2,4, 6-Tribromophenol 62 D 52-123 08129/19 12:28 09/17/19 16:18 4
2-Fluorobiphenyl 46 DX 47-119 08/29119 12:28 09117/19 16:18 4
Nitrobenzene-d5 69 D 45-113 08/29/19 12:28 09117/19 16:18 4
Terphenyl-d14 34 DX 50-123 08129/19 12:28 09/17119 16:18 4
Method: 245.1 -Mercury -Dissolved -Dissolved
Client Sample ID: C19081073-001C Lab Sample ID: 280-127755-1
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Mercury 3.7 0.20 0.027 ug/L 09/09/19 14:44 09/09/19 19:43 --1
Client Sample ID: C19081073-002C Lab Sample ID: 280-127755-4
Date Collected: 08/21/19 09:05 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Mercury ND 0.20 0.027 ug/L 09/09/19 14:44 09/09/19 19:45 --1
Client Sample ID: C19081073-003C Lab Sample ID: 280-127755-7
Date Collected: 08/21/19 09:20 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Mercury 0.20 0.20 0.027 ug/L 09/09/19 14:44 09/09/19 19:48 --1
Client Sample ID: C19081073-004C Lab Sample ID: 280-127755-10
Date Collected: 08/21/19 09:40 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Mercury 2.1 0.20 0.027 ug/L 09/09/19 14:44 09/09/19 19:50 1
Eurofins TestAmerica, Denver
Page 29 of 54 Page 75 c9/M/2019
Client Sample Results
Client: Energy Laboratories, Inc.
ProjecUSite: 11 (e) Byproduct Material
Method: 245.1 -Mercury -Dissolved -Dissolved
Client Sample ID: C19081073-005C
Date Collected: 08/21/19 09:45
Date Received: 08/28/19 10:45
Analyte
Mercury
Result Qualifier
1.4
RL
0.20
MDL Unit
0.027 ug/L
Job ID: 280-127755-1
Lab Sample ID: 280-127755-13
Matrix: Water
D Prepared Analyzed Dil Fae
09/09/1914:44 09/09/19 19:52 --1
Lab Sample ID: 280-127755-16
Matrix: Water
Client Sample ID: C19081073-006C
Date Collected: 08/21/19 10:15
Date Received: 08/28/19 10:45
Analyte
Mercury 0.46
RL MDL Unit D Prepared Analyzed Dil Fae I
-----0-.2-0 --0.-02-7 ug/L ---09/09/1914:44 09/09/1919:54 --1 .
Result Qualifier
Client Sample ID: C19081073-007C
Date Collected: 08/21/19 10:30
Date Received: 08/28/19 10:45
Result Qualifier Analyte
Mercury ----
Client Sample ID: C19081073-008C
Date Collected: 08/21/19 08:35
Date Received: 08/28/19 10:45
Analyte
Mercury
0.11 J
Result Qualifier
3.2
Client Sample ID: M3-54865
Date Collected: 08/23/19 11 : 20
Date Received: 08/28/19 10:45
Analyte
Mercury
Result Qualifier
---c-N=D
Lab Sample ID: 280-127755-19
Matrix: Water
RL MDL Unit D Prepared Analyzed Dil Fae
--0~.2~0 --0.~02=7 ug/L ---09/09/1914:44 09/09/1920:01 --1
RL MDL Unit
0.20 -~0.~02=7 -ug~/L __ _
RL MDL Unit
--=-=c ------,,---0.20 0.027 ug/L
Page 30 of 54
Lab Sample ID: 280-127755-22
Matrix: Water
D Prepared Analyzed Dil Fae
09/09/19 14:44 09/09119 20:03 --1
Lab Sample ID: 280-127755-25
Matrix: Water
D Prepared Analyzed Dil Fae
09/09/19 14:44 09/09/19 20:05 --1
Eurofins TestAmerica, Denver
Page 76 dJIM/2019
Surrogate Summary
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Method: 82608 -Volatile Organic Compounds (GC/MS)
Matrix: Water
Job ID: 280-127755-1
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
Lab Sample ID Client Sample ID
280-1277 55-3 C19081073-001F
280-127755-6 C 19081 073-002 F
280-127755-9 C19081073-003F
280-127755-12 C19081073-004F
280-127755-15 C19081073-005F
280-127755-18 C19081073-006F
280-127755-21 C19081073-007F
280-127755-24 C19081073-008F
LCS 280-469518/4 Lab Control Sample
LCSD 280-469518/5 Lab Control Sample Dup
MB 280-469518/8 Method Blank
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
TOL = Toluene-dB (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
DCA TOL BFB
(70-127) (80-125) (78-120)
97-96 ----"g3
96 96 95
97 95 93
98 96 93
97 98 93
99 96 93
98 97 93
99 97 94
97 96 95
96 95 94
97 97 94
Method: 8270C -Semivolatile Organic Compounds (GC/MS)
Matrix: Water
DBFM
(77-120)
99
99
100
99
98
98
100
99
102
101
100
Prep Type~_Total/NA
Percent Surrogate Recovery (Acceptance Limits)
Lab Sample ID
280-127755-2
280-127755-5
280-127755-8
280-127755-11
280-127755-11 -DL
280-127755-14
280-127755-17
280-127755-17 -DL
280-127755-20
280-127755-23
LCS 280-469200/2-A
LCSD 280-469200/3-A
MB 280-469200/1-A
Surrogate Legend
2FP = 2-Fluorophenol
PHL = Phenol-d5
Client Sample ID
C 19081073-0010
C19081073-002D
C19081073-003D
C 19081073-0040
C 19081073-0040
C19081073-005D
C19081073-006D
C 19081 073-0060
C19081073-0070
C19081073-0080
Lab Control Sample
Lab Control Sample Dup
Method Blank
TBP = 2,4,6-Tribromophenol
FBP = 2-Fluorobiphenyl
NBZ = Nitrobenzene-d5
TPHL = Terphenyl-d14
2FP
(17-71)
28
46
55
41
43 D
48
48
51 D
50
40
34
28
35
PHL
(10-52)
26
35
43
33
33 D
37
42
45 D
40
37
21
18
22
Page 31 of 54
TBP FBP NBZ TPHL
(52-123) (47-119) (45-113) (50-123)
34X 26X 36X 27X
76 60 74 68
78 63 75 72
65 56 73 31 X
61 D 59 D 71 D 34 DX
79 67 77 57
58 41 X 62 31 X
62 D 46 DX 69 D 34 DX
68 59 67 59
46X 32X 50 32X
78 69 74 82
64 54 59 68
70 60 71 81
Eurofins TestAmerica, Denver
Page 77 c9/2it/2019
I
QC Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
ProjecUSite: 11 (e) Byproduct Material
Method: 82608 -Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 280-469518/8
Matrix: Water
Analysis Batch: 469518
MB
Analyte Result
Tetrahydrofuran ND
MB
Surrogate %Recovery
1,2-Dichloroethane-d4 (Surr)
Toluene-dB (Surr)
4-Bromofluorobenzene (Surr)
Dibromof/uoromethane (Surr)
Lab Sample ID: LCS 280-469518/4
Matrix: Water
Analysis Batch: 469518
Analyte
Tetrahydrofuran
97
97
94
100
LCS LCS
MB
Qualifier
MB
Qualifier
Surrogate
1,2-Dichloroethane-d4 (Surr)
Toluene-dB (Surr)
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
%Recovery Qualifier
97
96
95
102
Lab Sample ID: LCSD 280-469518/5
Matrix: Water
Analysis Batch: 469518
Analyte
Tetrahydrofuran
Surrogate
1,2-Dichloroethane-d4 (Surr)
Toluene-dB (Surr)
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
LCSD LCSD
%Recovery Qualifier
~
95
94
101
RL
7.0
Limits
70-127
80-125
78-120
77-120
MDL Unit
2.0 ug/L
LCS LCS
D
Client Sample ID: Method Blank
Prep Type: Total/NA
Prepared Analyzed
09/03/19 09:10
Oil Fae --,
Prepared Analyzed Di/ Fae
09103/19 09:10 --1
09/03119 09:10 1
09/03/19 09:10 1
09103/19 09:10 1
Client Sample ID: Lab Control Sample m
Prep Type: Total/NA
Result Qualifier Unit
Spike
Added
50.0 ---4~0 . ...,.3 -ug~/L~--
D %Rec -~
%Rec.
Limits
42-136
Limits
70-127
80-125
78-120
77-120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD
Added Result Qualifier Unit
50.0 ---4~2~.8 -ug~/L~--
Limits
70-127
80-125
78-120
77-120
D %Rec
~
%Rec. RPO
Limits RPO Limit
42-136 -~6 -30
Method: 8270C -Semivolatile Organic Compounds (GC/MS)
Lab Sample ID: MB 280-469200/1-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 470328 Prep Batch: 469200
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fae
1, 1 '-Biphenyl ND 10 0.41 ug/L 08/29/19 12:28 09/12/19 15:26 ---1
1,2.4,5-Tetrachlorobenzene ND 10 0.24 ug/L 08/29/19 12:28 09/12/19 15:26 1
1,2,4-Trichlorobenzene ND 5.0 0.37 ug/L 08/29/19 12:28 09/12/19 15:26 1
1,2-Dichlorobenzene ND 5.0 0.30 ug/L 08/29/19 12:28 09/12119 15:26 1
1,3-Dichlorobenzene ND 10 2.0 ug/L 08/29/19 12:28 09112119 15:26
1,4-Dichlorobenzene ND 5.0 0.30 ug/L 08129119 12:28 09/12119 15:26
1,4-Dioxane ND 20 0.71 ug/L 08129/19 12:28 09112/19 15:26
Eurofins TestAmerica, Denver
Page 32 of 54 Page 78 <9/e4'2019
QC Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 280-469200/1-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 470328 Prep Batch: 469200
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
2,4,6-Trichlorophenol ND 10 0.74 µg/L 08/29119 12:28 09/1211915:26 ---1
2,4-Dichlorophenol ND 10 0.68 ug/L 08/29119 12:28 09112119 15:26
2,2'-oxybis[1-chloropropane] ND 10 0.42 ug/L 08129119 12:28 09/12/19 15:26
2 ,3 ,4,6-T etrachlorophenol ND 50 0.96 ug/L 08/29/19 12:28 09/12/19 15:26 1
2,4, 5-T richlorophenol ND 10 0.52 ug/L 08/29/19 12:28 09/12/19 15:26 1
2,4-Dimethylphenol ND 10 0.67 ug/L 08/29/19 12:28 09/12/19 15:26
2,4-Dinitrotoluene ND 10 0.93 ug/L 08/29/19 12:28 09/12/19 15:26
2,6-Dinitrotoluene ND 10 0.72 ug/L 08/29/19 12:28 09/12/19 15:26
2-Chloronaphthalene ND 4.0 0.46 ug/L 08/29/19 12:28 09/12/19 15:26 I 2-Chlorophenol ND 10 0.43 ug/L 08/29/19 12:28 09/12/19 15:26
2-Methylnaphthalene ND 4.0 0.41 ug/L 08/29/19 12:28 09/12/19 15:26
2-Methylphenol ND 10 0.56 ug/L 08/29/19 12:28 09/12/19 15:26
3 & 4 Methylphenol ND 10 1.0 ug/L 08/29/19 12:28 09/12/19 15:26
2-Nitroaniline ND 10 0.90 ug/L 08/29/19 12:28 09/12/19 15:26 1
2-Nitrophenol ND 10 0.62 ug/L 08/29/19 12:28 09/12/19 15:26 1
3,3'-Dichlorobenzidine ND 50 0.83 ug/L 08/29/19 12:28 09/12/19 15:26
3-Nitroaniline ND 10 0.78 ug/L 08/29/19 12:28 09/12/19 15:26
4,6-Dinitro-2-methylphenol ND 50 5.9 ug/L 08/29/19 12:28 09/12/19 15:26
4-Bromophenyl phenyl ether ND 10 0.41 ug/L 08/29/19 12:28 09/12/19 15:26
4-Chloro-3-methylphenol ND 10 0.45 ug/L 08/29/19 12:28 09/12/19 15:26
4-Chloroaniline ND 10 0.56 ug/L 08/29/19 12:28 09/12/19 15:26
4-Chlorophenyl phenyl ether ND 10 0.63 ug/L 08/29/19 12:28 09/12/19 15:26
4-Nitroaniline ND 10 0.84 ug/L 08/29/19 12:28 09/12/19 15:26
4-Nitrophenol ND 10 1.0 ug/L 08/29/19 12:28 09/12/19 15:26
Acenaphthene ND 4.0 0.45 ug/L 08/29/19 12:28 09/12/19 15:26
Acenaphthylene ND 4.0 0.50 ug/L 08/29/19 12:28 09/12/19 15:26
Acetophenone ND 10 0.52 ug/L 08/29/19 12:28 09/12/19 15:26
Anthracene ND 4.0 1.1 ug/L 08/29/19 12:28 09/12/19 15:26 1
Benzaldehyde ND 10 0.53 ug/L 08/29/19 12:28 09/12/19 15:26 1
Benzo[a]pyrene ND 4.0 0.64 ug/L 08/29/19 12:28 09/12/19 15:26
Benzo[b]fluoranthene ND 4.0 0.53 ug/L 08/29/19 12:28 09/12/19 15:26
Benzo[g,h,i]perylene ND 4.0 0.79 ug/L 08/29/1912:28 09/12/1915:26
Benzo[k]fluoranthene ND 4.0 0.56 ug/L 08/29/19 12:28 09/12/19 15:26
Benzo[a]anthracene ND 4.0 0.58 ug/L 08/29/19 12:28 09/12/19 15:26
Bis(2-chloroethoxy)methane ND 10 0.61 ug/L 08/29/19 12:28 09/12/19 15:26
Bis(2-chloroethyl)ether ND 10 0.49 ug/L 08/29/19 12:28 09/12/19 15:26
Bis(2-ethylhexyl) phthalate ND 10 1.1 ug/L 08/29/19 12:28 09/12/19 15:26
Butyl benzyl phthalate ND 5.0 2.0 ug/L 08/29/19 12:28 09/12/19 15:26
Caprolactam ND 10 2.7 ug/L 08/29/19 12:28 09/12/19 15:26
Carbazole ND 4.0 1.3 ug/L 08/29/19 12:28 09/12/19 15:26
Chrysene ND 4.0 0.52 ug/L 08/29/19 12:28 09/12/19 15:26
Dibenz(a,h)anthracene ND 4.0 0.65 ug/L 08/29/19 12:28 09/12/19 15:26
Di-n-butyl phthalate ND 4.0 0.88 ug/L 08/29/19 12:28 09/12/19 15:26
Di-n-octyl phthalate ND 5.0 1.6 ug/L 08/29/19 12:28 09/12/19 15:26
Dibenzofuran ND 4.0 0.36 ug/L 08/29/19 12:28 09/12/19 15:26
Diethyl phthalate ND 4.0 0.75 ug/L 08/29/19 12:28 09/12/19 15:26
Dimethyl phthalate ND 4.0 1.3 ug/L 08/29/19 12:28 09/12/19 15:26
Fluoranthene ND 4.0 0.64 ug/L 08/29/19 12:28 09/12/19 15:26
Fluorene ND 4.0 0.49 ug/L 08/29/19 12:28 09/12/19 15:26
Eurofins TestAmerica, Denver
Page 33 of 54 Page 79 c9/002019
QC Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 280-469200/1-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 470328 Prep Batch: 469200
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Hexachlorobenzene ND 10 0.96 ug/L 08/29/19 12:28 09/12/19 15:26 --1
Hexachlorobutadiene ND 30 7.5 ug/L 08/29/19 12:28 09/12/19 15:26
Hexachloroethane ND 30 7.6 ug/L 08/29/19 12:28 09/12/19 15:26
lndeno[1 ,2,3-cd]pyrene ND 5.0 1.6 ug/L 08/29/19 12:28 09/12/19 15:26
lsophorone ND 10 0.67 ug/L 08/29/19 12:28 09/12/19 15:26
N-Nitrosodi-n-propylamine ND 10 0.56 ug/L 08/29/19 12:28 09/12/19 15:26
n-Nitrosodiphenylamine(as ND 10 0.61 ug/L 08/29/19 12:28 09/12/19 15:26
diphenylamine)
Naphthalene ND 4.0 0.40 ug/L 08/29/19 12:28 09/12/19 15:26
m Nitrobenzene ND 10 0.43 ug/L 08/29/19 12:28 09/12/19 15:26
Pentachlorophenol ND 50 5.5 ug/L 08/29/19 12:28 09/12/19 15:26
Phenanthrene ND 4.0 0.28 ug/L 08/29/19 12:28 09/12/19 15:26
Phenol ND 10 0.56 ug/L 08/29/19 12:28 09/12/19 15:26
Pyrene ND 10 0.43 ug/L 08/29/19 12:28 09/12/19 15:26
1,3-Dinitrobenzene ND 10 0.97 ug/L 08/29/19 12:28 09/12/19 15:26
1-Methylnaphthalene ND 4.0 0.35 ug/L 08/29/19 12 :28 09/12/19 15:26
2,6-Dichlorophenol ND 10 0.75 ug/L 08/29/19 12:28 09/12/19 15:26
Aniline ND 10 0.88 ug/L 08/29/19 12:28 09/12/19 15:26
Azobenzene ND 4.0 0.54 ug/L 08/29/19 12:28 09/12/19 15:26
Benzidine ND 100 4.4 ug/L 08/29/19 12:28 09/12/19 15:26
Benzyl alcohol ND 10 0.35 ug/L 08/29/19 12:28 09/12/19 15:26
Diphenylamine ND 10 0.49 ug/L 08/29/19 12:28 09/12/19 15:26
Hexadecane ND 10 0.35 ug/L 08/29/19 12:28 09/12/19 15:26
N-Nitrosodimethylamine ND 10 0.62 ug/L 08/29/19 12:28 09/12/19 15:26
Pyridine ND 20 5.0 ug/L 08/29/19 12:28 09/12/19 15:26
1,2-Diphenylhydrazine(as ND 10 0.54 ug/L 08/29/19 12:28 09/12/19 15:26
Azobenzene)
3-Methylphenol ND 10 0.40 ug/L 08/29/19 12:28 09/12/19 15:26
4-Methylphenol ND 10 1.0 ug/L 08/29/19 12:28 09/12/19 15:26
Alachlor ND 20 0.60 ug/L 08/29/19 12:28 09/12/19 15:26
Famphur ND 100 0.80 ug/L 08/29/19 12:28 09/12/19 15:26
lndene ND 10 0.82 ug/L 08/29/19 12:28 09/12/19 15:26
Total Cresols ND 10 0.40 ug/L 08/29/19 12:28 09/12/19 15:26
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed DII Fae
2-F/uorophenol 35 17 -71 08/29119 12:28 09/12119 15:26 ---1
Phenol-d5 22 10-52 08129/19 12:28 09/12119 15:26 1
2, 4, 6-Tribromophenol 70 52-123 08/29119 12:28 09112/19 15:26 1
2-Fluorobiphenyl 60 47-119 08129/19 12:28 09/12/19 15:26
Nitrobenzene-d5 71 45. 113 08/29119 12:28 09112/19 15:26 1
Terphenyl-d14 81 50-123 08/29/19 12:28 09/12119 15.·26 1
Lab Sample ID: LCS 280-469200/2-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 470328 Prep Batch: 469200
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
1, 1 '-Biphenyl 70.0 43.0 ug/L -~ 53-116 ----
1,2,4,5-Tetrachlorobenzene 70.0 37.9 ug/L 54 52 .100
Eurofins TestAmerica, Denver
Page 34 of 54 Page 80 c9/QJt/2019
QC Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
ProjecUSite: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 280-469200/2-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 470328 Prep Batch: 469200
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
1,2 ,4-T richlorobenzene 70.0 28.9 * ug/L ---;n-47 -103 ----
1,2-Dichlorobenzene 70.0 29.9 * ug/L 43 44-103
1,3-Dichlorobenzene 70.0 27.3 * ug/L 39 42-100
1,4-Dichlorobenzene 70.0 28.3 * ug/L 40 43-101
1,4-Dioxane 70.0 22.5 ug/L 32 20-63
2,4,6-Trichlorophenol 70.0 60.0 ug/L 86 52 -132
2,4-Dichlorophenol 70.0 60.2 ug/L 86 60-108
2,2'-oxybis[1-chloropropane] 70.0 65.7 ug/L 94 49 -114
2,3,4,6-Tetrachlorophenol 70.0 58.9 ug/L 84 53-129
2,4,5-Trichlorophenol 70.0 57.9 ug/L 83 51 -121
2,4-Dimethylphenol 70.0 56.5 ug/L 81 54-105
2,4-Dinitrotoluene 70.0 63.5 ug/L 91 52-134
2,6-Dinitrotoluene 70.0 62.7 ug/L 90 52-132
2-Chloronaphthalene 70.0 40.5 ug/L 58 52-116
2-Chlorophenol 70.0 48.4 ug/L 69 50-105
2-Methylnaphthalene 70.0 39.2 ug/L 56 55 _ 101
2-Methylphenol 70.0 41 .8 ug/L 60 43_94
3 & 4 Methylphenol 70.0 39.5 ug/L 56 34-88
2-Nitroaniline 70.0 64.5 ug/L 92 42-142
2-Nitrophenol 70.0 55.4 ug/L 79 58-110
3,3'-Dichlorobenzidine 160 122 ug/L 76 56-112
3-Nitroaniline 70.0 52.5 ug/L 75 34 _ 118
4,6-Dinitro-2-methylphenol 140 123 ug/L 88 66-126
4-Bromophenyl phenyl ether 70.0 59.3 ug/L 85 60-109
4-Chloro-3-methylphenol 70.0 63.1 ug/L 90 63-107
4-Chloroaniline 70.0 51 .8 ug/L 74 41 _ 93
4-Chlorophenyl phenyl ether 70.0 56.1 ug/L 80 57 -120
4-Nitroaniline 70.0 59.3 ug/L 85 55 _ 123
4-Nitrophenol 140 51 .1 ug/L 37 15-60
Acenaphthene 70.0 51 .5 ug/L 74 52-122
Acenaphthylene 70.0 48.5 ug/L 69 58-112
Acetophenone 70.0 56.1 ug/L 80 58-108
Anthracene 70.0 61 .1 ug/L 87 62-113
Benzaldehyde 80.0 37.2 ug/L 47 25-91
Benzo[a]pyrene 70.0 59.4 ug/L 85 61-114
Benzo[b ]fluoranthene 70.0 62.0 ug/L 89 61-110
Benzo[g, h, i]perylene 70.0 61 .0 ug/L 87 67 -111
Benzo[k]fluoranthene 70.0 60.9 ug/L 87 69-119
Benzo[a]anthracene 70.0 60.4 ug/L 86 55-115
Bis(2-chloroethoxy)methane 70.0 52.7 ug/L 75 61 -107
Bis(2-chloroethyl)ether 70.0 49.9 ug/L 71 56-112
Bis(2-ethylhexyl) phthalate 70.0 60.2 ug/L 86 60-116
Butyl benzyl phthalate 70.0 60.2 ug/L 86 57 -111
Caprolactam 80.0 15.0 ug/L 19 10-50
Carbazole 70.0 61 .6 ug/L 88 69-109
Chrysene 70.0 59.1 ug/L 84 63 -118
Dibenz(a,h)anthracene 70.0 63.3 ug/L 90 65 -111
Di-n-butyl phthalate 70.0 63.3 ug/L 90 68-110
Di-n-octyl phthalate 70.0 62.6 ug/L 89 49 _ 111
Eurofins TestAmerica, Denver
Page 35 of 54 Page 81 c91M/2019
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
QC Sample Results
Job ID: 280-127755-1
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 280-469200/2-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 470328 Prep Batch: 469200
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Dibenzofuran 70.0 52.9 ug/L ~ 58-116 ----
Diethyl phthalate 70.0 66.4 ug/L 95 57 -121
Dimethyl phthalate 70.0 64.2 ug/L 92 56-120
Fluoranthene 70.0 63.0 ug/L 90 68-111
Fluorene 70.0 59.4 ug/L 85 56-119
Hexachlorobenzene 70.0 59.7 ug/L 85 64-112
Hexachlorobutadiene 70.0 23.9 J * ug/L 34 41 -102
Hexachloroethane 70.0 22.4 J ug/L 32 31 -100
lndeno[1,2,3-cd]pyrene 70.0 62.3 ug/L 89 56-100
lsophorone 70.0 59.0 ug/L 84 59-100
N-Nitrosodi-n-propylamine 70.0 60.1 ug/L 86 59-106
n-Nitrosodiphenylamine(as 70.0 60.8 ug/L 87 64-112
diphenylamine)
Naphthalene 70.0 39.7 ug/L 57 53-105
Nitrobenzene 70.0 56.9 ug/L 81 56-106
Pentachlorophenol 140 94.9 ug/L 68 48-121
Phenanthrene 70.0 61 .7 ug/L 88 63-113
Phenol 70.0 18.3 ug/L 26 11 -52
Pyrene 70.0 58.3 ug/L 83 62-114
1,3-Dinitrobenzene 70.0 64.0 ug/L 91 66-124
1-Methylnaphthalene 70.0 40.9 ug/L 58 57 -100
2,6-Dichlorophenol 70.0 60.5 ug/L 86 56-104
Aniline 70.0 37.9 ug/L 54 16-94
Azobenzene 70.0 57.1 ug/L 82 59-124
Benzidine 160 56.1 J ug/L 35 5_93
Benzyl alcohol 70.0 40.4 ug/L 58 34-91
Diphenylamine 59.5 52.5 ug/L 88 62-118
Hexadecane 70.0 57.3 ug/L 82 23-134
N-Nitrosodimethylamine 70.0 24.2 ug/L 35 13-70
Pyridine 140 43.5 ug/L 31 10-69
1,2-Diphenylhydrazine(as 70.8 57.7 ug/L 82 59-124
Azobenzene)
3-Methylphenol 70.0 39.5 ug/L 56 34-88
4-Methylphenol 70.0 39.5 ug/L 56 34-88
lndene 80.0 36.2 * ug/L 45 46-108
Total Cresols 140 81.3 ug/L 58
LCS LCS
Surrogate %Recovery Qualifier Limits
2-Fluorophenol 34 17 -71
Phenol-d5 21 10-52
2, 4, 6-Tribromophenol 78 52-123
2-Fluorobiphenyl 69 47-119
Nitrobenzene-d5 74 45-113
Terpheny/-d14 82 50-123
Eurofins TestAmerica, Denver
Page 36 of 54 Page 82 <9/M/2019
QC Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 ( e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 280-469200/3-A Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 470328 Prep Batch: 469200
Spike LCSO LCSO %Rec. RPO
Analyte Added Result Qualifier Unit 0 %Rec Limits RPO Limit
1, 1 '-Biphenyl 70.0 34.2 .---ug~ 49 53 _ 116 -23 31
1,2,4,5-Tetrachlorobenzene 70.0 29.6 * ug/L 42 52-100 25 32
1,2,4-Trichlorobenzene 70.0 22.3 * ug/L 32 47 -103 26 42
1,2-Dichlorobenzene 70.0 24.2 * ug/L 35 44-103 21 44
1,3-Dichlorobenzene 70.0 21 .7 * ug/L 31 42-100 23 46
1,4-Dichlorobenzene 70.0 22.9 * ug/L 33 43-101 21 45
1,4-Dioxane 70.0 18.3 J ug/L 26 20-63 21 35
2,4,6-Trichlorophenol 70.0 49.7 ug/L 71 52-132 19 32
2,4-Dichlorophenol 70.0 47.2 ug/L 67 60-108 24 34 ~ 2,2'-oxybis[1-chloropropane] 70.0 54.8 ug/L 78 49-114 18 35
2,3 ,4 ,6-T etrachlorophenol 70.0 47.4 J ug/L 68 53-129 22 36
2,4,5-Trichlorophenol 70.0 47.1 ug/L 67 51-121 20 33
2,4-Dimethylphenol 70.0 49.1 ug/L 70 54 _ 105 14 31
2,4-Dinitrotoluene 70.0 52.2 ug/L 75 52-134 19 34
2,6-Dinitrotoluene 70.0 50.8 ug/L 73 52-132 21 37
2-Chloronaphthalene 70.0 31 .8 • ug/L 45 52-116 24 31
2-Chlorophenol 70.0 40.7 ug/L 58 50-105 17 36
2-Methylnaphthalene 70.0 30.5 • ug/L 44 55-101 25 33
2-Methylphenol 70.0 36.2 ug/L 52 43_94 14 33
3 & 4 Methylphenol 70.0 33.6 ug/L 48 34-88 16 32
2-Nitroaniline 70.0 54.3 ug/L 78 42-142 17 34
2-Nitrophenol 70.0 44.7 ug/L 64 58-110 21 39
3,3'-Dichlorobenzidine 160 101 ug/L 63 56-112 18 50
3-Nitroaniline 70.0 45.8 ug/L 65 34 _ 118 14 38
4,6-Dinitro-2-methylphenol 140 99.5 ug/L 71 66-126 21 39
4-Bromophenyl phenyl ether 70.0 46.9 ug/L 67 60-109 23 31
4-Chloro-3-methylphenol 70.0 52.5 ug/L 75 63-107 18 35
4-Chloroaniline 70.0 44.8 ug/L 64 41 _ 93 14 49
4-Chlorophenyl phenyl ether 70.0 46.0 ug/L 66 57 -120 20 33
4-Nitroaniline 70.0 50.7 ug/L 72 55-123 16 35
4-Nitrophenol 140 44.1 ug/L 32 15-60 15 34
Acenaphthene 70.0 42.1 ug/L 60 52-122 20 30
Acenaphthylene 70.0 39.9 * ug/L 57 58-112 20 31
Acetophenone 70.0 46.5 ug/L 66 58-108 19 34
Anthracene 70.0 49.1 ug/L 70 62-113 22 31
Benzaldehyde 80.0 35.6 ug/L 45 25-91 4 42
Benzo[a]pyrene 70.0 48.5 ug/L 69 61-114 20 33
Benzo[b Jfluoranthene 70.0 50.3 ug/L 72 61 -110 21 37
Benzo[g ,h,i]perylene 70.0 50.5 ug/L 72 67 -111 19 33
Benzo[k]fluoranthene 70.0 49.2 ug/L 70 69-119 21 31
Benzo[a]anthracene 70.0 48.8 ug/L 70 55-115 21 33
Bis(2-chloroethoxy)methane 70.0 43.3 ug/L 62 61 -107 20 34
Bis(2-chloroethyl)ether 70.0 41 .7 ug/L 60 56-112 18 36
Bis(2-ethylhexyl) phthalate 70.0 48.9 ug/L 70 60-116 21 35
Butyl benzyl phthalate 70.0 49.0 ug/L 70 57 -111 21 33
Caprolactam 80.0 12.8 ug/L 16 10-50 15 35
Carbazole 70.0 49.9 ug/L 71 69-109 21 31
Chrysene 70.0 48.1 ug/L 69 63-118 20 32
Eurofins TestAmerica, Denver
Page 37 of 54 Page 83 <9/QR/2019
QC Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Method: 8270C -Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 280-469200/3-A Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 470328 Prep Batch: 469200
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
Dibenz(a,h)anthracene 70.0 53.1 ug/L -~ 65 -111 --18 ~
Di-n-butyl phthalate 70.0 49.4 ug/L 71 68-110 25 30
Di-n-octyl phthalate 70.0 50.2 ug/L 72 49 -111 22 30
Dibenzofuran 70.0 43.4 ug/L 62 58-116 20 31
Diethyl phthalate 70.0 54.9 ug/L 78 57 -121 19 34
Dimethyl phthalate 70.0 52.7 ug/L 75 56-120 20 32
Fluoranthene 70.0 49.9 ug/L 71 68-111 23 33
Fluorene 70.0 48.4 ug/L 69 56-119 20 30
Hexachlorobenzene 70.0 47.7 ug/L 68 64-112 22 33 I Hexachlorobutadiene 70.0 17.2 J. ug/L 25 41 -102 33 49
Hexachloroethane 70.0 17.4 J. ug/L 25 31 -100 25 50
lndeno[1,2,3-cd]pyrene 70.0 51.1 ug/L 73 56-100 20 37
lsophorone 70.0 47.6 ug/L 68 59-100 22 32
N-Nitrosodi-n-propylamine 70.0 48.8 ug/L 70 59-106 21 33
n-Nitrosodiphenylamine(as 70.0 50.2 ug/L 72 64 -112 19 33
diphenylamine)
Naphthalene 70.0 31.9 * ug/L 46 53-105 22 35
Nitrobenzene 70.0 46.6 ug/L 67 56-106 20 34
Pentachlorophenol 140 74.1 ug/L 53 48-121 25 35
Phenanthrene 70.0 49.1 ug/L 70 63-113 23 31
Phenol 70.0 15.1 ug/L 22 11 -52 19 34
Pyrene 70.0 48.4 ug/L 69 62-114 18 31
1,3-Dinitrobenzene 70.0 52.1 ug/L 74 66-124 20 37
1-Methylnaphthalene 70.0 31 .9 * ug/L 46 57 -100 25 32
2,6-Dichlorophenol 70.0 47.4 ug/L 68 56-104 24 33
Aniline 70.0 32.4 ug/L 46 16-94 16 45
Azobenzene 70.0 46.9 ug/L 67 59-124 19 31
Benzidine 160 61.2 J ug/L 38 5_ 93 9 50
Benzyl alcohol 70.0 33.7 ug/L 48 34-91 18 35
Diphenylamine 59.5 44.1 ug/L 74 62-118 17 50
Hexadecane 70.0 46.5 ug/L 66 23-134 21 31
N-Nitrosodimethylamine 70.0 21 .1 ug/L 30 13-70 14 37
Pyridine 140 31.3 * ug/L 22 10-69 33 26
1,2-Diphenylhydrazine(as 70.8 47.5 ug/L 67 59 _ 124 19 30
Azobenzene)
3-Methylphenol 70.0 33.6 ug/L 48 34-88 16 32
4-Methylphenol 70.0 33.6 ug/L 48 34-88 16 32
lndene 80.0 30.6 * ug/L 38 46-108 17 40
Total Cresols 140 69.8 ug/L 50 15
LCSD LCSD
Surrogate %Recovery Qualifier Limits
2-Fluorophenol 28 17-71
Phenol-d5 18 10-52
2, 4, 6-Tribromophenol 64 52-123
2-Fluorobiphenyl 54 47 -119
Nitrobenzene-d5 59 45-113
Terphenyl-d14 68 50-123
Eurofins TestAmerica, Denver
Page 38 of 54 Page 84 c9@tf2019
QC Sample Results
Client: Energy Laboratories, Inc.
Project/Site: 11 ( e) Byproduct Material
Method: 245.1 -Mercury -Dissolved
Lab Sample ID: MB 280-470040/1-A
Matrix: Water
Analysis Batch: 470161
MB MB
Analyte
Mercury
Result Qualifier
---N-D
Lab Sample ID: LCS 280-470040/2-A
Matrix: Water
Analysis Batch: 470161
RL
0.20
MDL Unit
--0.-027 ug/L
Spike LCS LCS
Job ID: 280-127755-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 470040
D Prepared Analyzed Dil Fae
09/09/19 14:44 09/09/1919:39 --1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 470040
Added Result Qualifier Unit D %Rec Analyte
Mercury -----s:o5 -~ -ug-/L---~
%Rec.
Limits
90 -110
Eurofins TestAmerica, Denver
Page 39 of 54 Page 85 c9@t12019
QC Association Summary
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
GC/MS VOA
Analysis Batch: 469518
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
280-127755-3 C19081073-001 F Total/NA Water 8260B
280-127755-6 C19081073-002F Total/NA Water 8260B
280-127755-9 C 19081073-003F Total/NA Water 8260B
280-127755-12 C 19081073-004F Total/NA Water 8260B
280-127755-15 C 19081073-005F Total/NA Water 8260B
280-127755-18 C 19081073-006F Total/NA Water 82608
280-1277 55-21 C19081073-007F Total/NA Water 82608
280-127755-24 C 19081073-008F Total/NA Water 8260B
MB 280-469518/8 Method Blank Total/NA Water 8260B
LCS 280-469518/4 Lab Control Sample Total/NA Water 8260B
LCSD 280-469518/5 Lab Control Sample Dup Total/NA Water 8260B
GC/MS Semi VOA
Prep Batch: 469200
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
280-127755-2 C 19081073-001 D Total/NA Water 3510C
280-127755-5 C19081073-002D Total/NA Water 3510C E 280-127755-8 C 19081073-003D Total/NA Water 3510C
280-127755-11 C 19081073-004D Total/NA Water 3510C
280-127755-11 -DL C19081073-004D Total/NA Water 3510C
280-127755-14 C19081073-005D Total/NA Water 3510C
280-127755-17 -DL C19081073-006D Total/NA Water 3510C
280-127755-17 C 19081 073-006D Total/NA Water 3510C
280-127755-20 C 19081073-007D Total/NA Water 3510C
280-127755-23 C 19081073-008D Total/NA Water 3510C
MB 280-469200/1-A Method Blank Total/NA Water 3510C
LCS 280-469200/2-A Lab Control Sample Total/NA Water 3510C
LCSD 280-469200/3-A Lab Control Sample Dup Total/NA Water 3510C
Analysis Batch: 470328
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
280-127755-2 C 19081073-001D Total/NA Water 8270C 469200
280-127755-5 C 19081 073-0020 Total/NA Water 8270C 469200
280-1277 55-8 C19081073-003D Total/NA Water 8270C 469200
280-1277 55-11 C 19081073-004D Total/NA Water 8270C 469200
280-127755-14 C 19081073-005D Total/NA Water 8270C 469200
280-127755-17 C 19081 073-006D Total/NA Water 8270C 469200
280-127755-20 C 19081073-007D Total/NA Water 8270C 469200
280-127755-23 C19081073-008D Total/NA Water 8270C 469200
MB 280-469200/1-A Method Blank Total/NA Water 8270C 469200
LCS 280-469200/2-A Lab Control Sample Total/NA Water 8270C 469200
LCSD 280-469200/3-A Lab Control Sample Dup Total/NA Water 8270C 469200
Analysis Batch: 470907
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
280-127755-11 -DL C 19081073-004D Total/NA Water 8270C 469200
280-127755-17 -DL C19081073-006D Total/NA Water 8270C 469200
Eurofins TestAmerica, Denver
Page 40 of 54 Page 86 c9~2019
QC Association Summary
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
-------Metals
Prep Batch: 470040
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
280-127755-1 C19081073-001C Dissolved Water 245.1
280-127755-4 C 19081073-002C Dissolved Water 245.1
280-127755-7 C 19081073-003C Dissolved Water 245.1
280-127755-10 C 19081073-004C Dissolved Water 245.1
280-127755-13 C 19081073-005C Dissolved Water 245.1
280-127755-16 C 19081073-006C Dissolved Water 245.1
280-127755-19 C19081073-007C Dissolved Water 245.1
280-127755-22 C 19081073-008C Dissolved Water 245.1
280-127755-25 M3-54865 Dissolved Water 245.1
MB 280-470040/1-A Method Blank Total/NA Water 245.1
LCS 280-470040/2-A Lab Control Sample Total/NA Water 245.1
Analysis Batch: 470161
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
280-127755-1 C19081073-001C Dissolved Water 245.1 470040
280-127755-4 C 19081073-002C Dissolved Water 245.1 470040
280-127755-7 C 19081073-003C Dissolved Water 245.1 470040
280-127755-10 C 19081073-004C Dissolved Water 245.1 470040
280-127755-13 C 19081073-005C Dissolved Water 245.1 470040
280-127755-16 C 19081073-006C Dissolved Water 245.1 470040
280-127755-19 C 19081073-007C Dissolved Water 245.1 470040
280-127755-22 C 19081073-008C Dissolved Water 245.1 470040
280-127755-25 M3-54865 Dissolved Water 245.1 470040
MB 280-470040/1-A Method Blank Total/NA Water 245.1 470040
LCS 280-470040/2-A Lab Control Sample Total/NA Water 245.1 470040
Eurofins TestAmerica, Denver
Page 41 of 54 Page 87 c9~2019
Lab Chronicle
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Client Sample ID: C19081073-001C Lab Sample ID: 280-127755-1
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch DII Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 245.1 30 ml 50 m---C--470040 09/09/19 14:44 MRJ TAL DEN
Dissolved Analysis 245.1 470161 09/09/19 19:43 MRJ TAL DEN
Client Sample ID: C19081073-001 D Lab Sample ID: 280-127755-2
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 3510C 996.8 ml 1 ml 469200 08/29/19 12:28 AZG TAL DEN
Total/NA Analysis 8270C 470328 09/12/19 20:21 AJE TAL DEN
Client Sample ID: C19081073-001F Lab Sample ID: 280-127755-3
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45 ! Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 82608 5 5 ml 5 ~ 469518 09/03/19 14:28 TAW TAL DEN
Client Sample ID: C19081073-002C Lab Sample ID: 280-127755-4
Date Collected: 08/21/19 09:05 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 245.1 30 ml 50 ml 470040 09/09/19 14:44 MRJ TAL DEN
Dissolved Analysis 245.1 470161 09/09/19 19:45 MRJ TAL DEN
Client Sample ID: C19081073-002D Lab Sample ID: 280-127755-5
Date Collected: 08/21/19 09:05 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab -----Total/NA Prep 3510C 1084.7 ml 1 ml 469200 08/29/19 12:28 AZG TAL DEN
Total/NA Analysis 8270C 470328 09/12/19 20:51 AJE TAL DEN
Client Sample ID: C19081073-002F Lab Sample ID: 280-127755-6
Date Collected: 08/21/19 09:05 Matrix: Water
Date Received: 08/28/1910:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 82608 -----5 5 ml 5 ml 469518 09/03/19 14:50 TAW TAL DEN
Eurofins TestAmerica, Denver
Page 42 of 54 Page 88 c9/eitl2019
Lab Chronicle
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Client Sample ID: C19081073-003C Lab Sample ID: 280-127755-7
Date Collected: 08/21/19 09:20 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Oil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 245.1 30 ml 50 ml 470040 09/09/19 14:44 MRJ TAl DEN
Dfssolved Analysis 245.1 470161 09/09/19 19:48 MRJ TAl DEN
Client Sample ID: C19081073-003D Lab Sample ID: 280-127755-8
Date Collected: 08/21/19 09:20 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 3510C 1117.2 ml 1 ml 469200 08/29/19 12:28 AZ.G TAl DEN
Total/NA Analysis 8270C 470328 09/12/19 21 :20 AJE TAl DEN
Client Sample ID: C19081073-003F Lab Sample ID: 280-127755-9
Date Collected: 08/21/19 09:20 Matrix: Water
Date Received: 08/28/19 10:45 ! Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 82608 --5 5ml 5 ml 469518 09/03/19 15: 11 TAW TAlDEN
Client Sample ID: C19081073-004C Lab Sample ID: 280-127755-10
Date Collected: 08/21 /19 09:40 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Oil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 245.1 30 ml 50 ml 470040 09/09/19 14:44 MRJ TAl DEN
Dissolved Analysis 245.1 470161 09/09/19 19:50 MRJ TAl DEN
Client Sample ID: C19081073-004D Lab Sample ID: 280-127755-11
Date Collected: 08/21/19 09:40 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 3510C 1076.6 ml 1 ml 469200 08/29/19 12:28 AZ.G TAl DEN
Total/NA Analysis 8270C 470328 09/12/19 21 :49 AJE TAl DEN
Total/NA Prep 3510C Dl 1076.6 ml 1 ml 469200 08/29/19 12:28 AZ.G TAl DEN
Total/NA Analysis 8270C Dl 4 470907 09/17/19 15:48 AJE TAl DEN
Client Sample ID: C19081073-004F Lab Sample ID: 280-127755-12
Date Collected: 08/21/19 09:40 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch DII Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 82608 --5 5ml 5 ml 469518 09/03/19 15:32 TAW TAl DEN
Eurofins TestAmerica, Denver
Page 43 of 54 Page 89 c91PR/2019
Lab Chronicle
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Client Sample ID: C19081073-005C Lab Sample ID: 280-127755-13
Date Collected: 08/21/19 09 :45 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Oil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 245.1 30 ml 50 ml 470040 09/09/19 14:44 MRJ TAL DEN
Dissolved Analysis 245.1 470161 09/09/19 19:52 MRJ TAL DEN
Client Sample ID: C19081073-0050 Lab Sample ID: 280-127755-14
Date Collected: 08/21/19 09 :45 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Oil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 3510C 1084.3 ml 1 ml 469200 08/29/19 12:28 AZG TAL DEN
Total/NA Analysis 8270C 470328 09/12/19 22:19 AJE TAL DEN
Client Sample ID: C19081073-005F Lab Sample ID: 280-127755-15
Date Collected: 08/21/19 09:45 Matrix: Water
Date Received: 08/28/19 10:45 m Batch Batch Oil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 82608 ----5 5ml 5ml 469518 09/03/19 15:53 TAW TAL DEN
Client Sample ID: C19081073-006C Lab Sample ID: 280-127755-16
Date Collected: 08/21/19 10:15 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Oil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 245.1 ----30 ml 50 ml 470040 09/09/19 14:44 MRJ TAL DEN
Dissolved Analysis 245.1 470161 09/09/19 19:54 MRJ TAL DEN
Client Sample ID: C19081073-0060 Lab Sample ID: 280-127755-17
Date Collected: 08/21/19 10:15 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Oil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab ----Total/NA Prep 3510C 1141 .5 ml 1 ml 469200 08/29/19 12:28 AZG TAL DEN
Total/NA Analysis 8270C 470328 09/12/19 22:48 AJE TAL DEN
Total/NA Prep 3510C DL 1141.5 ml 1 ml 469200 08/29/19 12:28 AZG TAL DEN
Total/NA Analysis 8270C DL 4 470907 09/17/1916:18 AJE TAL DEN
Client Sample ID: C19081073-006F Lab Sample ID: 280-127755-18
Date Collected: 08/21/19 10:15 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 82608 --5 5ml 5ml 469518 09/03/19 16: 14 TAW TAL DEN
Eurofins TestAmerica, Denver
Page 44 of 54 Page 90 c9/002019
Lab Chronicle
Client: Energy Laboratories, Inc. Job ID: 280-127755-1
Project/Site: 11 (e) Byproduct Material
Client Sample ID: C19081073-007C Lab Sample ID: 280-127755-19
Date Collected: 08/21/19 10:30 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 245~1-30 ml 50ml-470040 09/09/19 14:44 MRJ TAl DEN
Dissolved Analysis 245.1 470161 09/09/19 20:01 MRJ TAl DEN
Client Sample ID: C19081073-007D Lab Sample ID: 280-127755-20
Date Collected: 08/21/19 10:30 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 3510C 1100.7ml 1 ml -469200 08/29/19 12:28 AZG TAl DEN
Total/NA Analysis 8270C 470328 09/12/19 23:17 AJE TAl DEN
Client Sample ID: C19081073-007F Lab Sample ID: 280-127755-21
Date Collected: 08/21/19 10:30 Matrix: Water
Date Received: 08/28/1910:45 m Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 82608 --5 5 ml 5 ml 46~ 09/03/19 16:35 TAW TAl DEN
Client Sample ID: C19081073-008C Lab Sample ID: 280-127755-22
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45 -
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab -----Dissolved Prep 245.1 30ml 50ml 470040 09/09/19 14:44 MRJ TAl DEN
Dissolved Analysis 245.1 470161 09/09/19 20:03 MRJ TAl DEN
Client Sample ID: C19081073-008D Lab Sample ID: 280-127755-23
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 3510C 1012.8 ml 1 ml 469200 08/29/19 12:28 AZG TAl DEN
Total/NA Analysis 8270C 470328 09/12/19 23:4 7 AJE TAL DEN
Client Sample ID: C19081073-008F Lab Sample ID: 280-127755-24
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 82608 --5 5 ml 5 ml 469518 09/03/19 16:57 TAW TAl DEN
Eurofins TestAmerica, Denver
Page 45 of 54 Page 91 c9/002019
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Client Sample ID: M3-54865
Date Collected: 08/23/19 11 : 20
Date Received: 08/28/19 10:45
Batch
Prep Type Type
Dissolv-ed.,_--Prep
Dissolved Analysis
Laboratory References:
Batch
Method
245.1 ---
245.1
Lab Chronicle
Oil
Run Factor
Initial
Amount
30 ml
Final
Amount
50ml
TAL DEN= Eurofins TestAmerica, Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL (303}736-0100
Page 46 of 54
Job ID: 280-127755-1
Lab Sample ID: 280-127755-25
Matrix: Water
Batch Prepared
Number or Analyzed Analyst Lab
470040 09/09/19 14:44 MRJ =-TA~L~D=E~N-
470161 09/09/19 20:05 MRJ TAL DEN
Eurofins TestAmerica, Denver
Page 92 c9/1?R/2019
Accreditation/Certification Summary
Client: Energy Laboratories, Inc.
ProjecUSite: 11 (e) Byproduct Material
Laboratory: Eurofins TestAmerica, Denver
Job ID: 280-127755-1
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
A2LA Dept. of Defense ELAP 2907.01 10-31-19
A2LA DoD 2907.01 10-31-19
A2LA ISO/IEC 17025 2907.01 10-31-19
A2LA ISO/IEC 17025 2907.01 10-31-19
Alabama State Program 40730 09-30-12 *
Alaska (UST) State 18-001 01-08-20
Alaska (UST) State Program UST-30 01-08-20
Arizona State AZ0713 12-20-19
Arizona State Program AZ0713 12-20-19
Arkansas DEQ State 19-047-0 06-01-20
Arkansas DEQ State Program 88-0687 06-01-20
California State 2513 01-08-20
California State Program 2513 01-08-20
Connecticut State PH-0686 09-30-20
Connecticut State Program PH-0686 09-30-20
Florida NELAP E87667 06-30-20
Florida NELAP E87667-57 06-30-20
Georgia State Program NIA 01-08-20
Illinois NELAP 200017 04-30-20
Illinois NELAP 2000172019-1 04-30-20
Iowa State Program 370 12-01-20
Kansas NELAP E-10166 04-30-20
Louisiana NELAP 02096 06-30-20
Louisiana NELAP 30785 06-30-20
Maine State Program C00002 03-03-21
Minnesota NELAP 8-999-405 12-31-19
Minnesota NELAP 1545373 08-05-20
Minnesota NELAP 1545373 12-31-19
Nevada State C0000262020-1 09-18-19
Nevada State Program C00026 07-31-20
New Hampshire NELAP 205310 04-28-20
New Jersey NELAP C0004 06-30-20
New Jersey NELAP 190002 06-30-20
New York NELAP 11964 04-01-20
New York NELAP 59923 04-01-20
North Carolina (VWv/SW) State Program 358 12-31-19
North Dakota State Program R-034 01-08-20
Oklahoma State Program 8614 08-31-20
Oregon NELAP 4025 01-08-20
Oregon NELAP 4025-011 01-08-20
Pennsylvania NELAP 68-00664 07-31-20
Pennsylvania NELAP 013 08-01-20
South Carolina State Program 72002001 01-08-20
Texas NELAP T104704183-18-15 09-30-19
Texas NELAP T104704183-18-15 09-30-19
US Fish & Wildlife Federal 07-31-20
USDA Federal 03-26-21
Utah NELAP C000026 07-31-20
Utah NELAP C0000262019-11 07-31-20
Virginia NELAP 460232 06-14-20
* Accreditation/Certification renewal pending -accreditation/certification considered valid.
Eurofins TestAmerica, Denver
Page 47 of 54 Page 93 <9/002019
Accreditation/Certification Summary
Client: Energy Laboratories, Inc.
ProjecUSite: 11 (e) Byproduct Material
Laboratory: Eurofins TestAmerica, Denver (Continued)
Job ID: 280-127755-1
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
Virginia NELAP 10490 06-14-20
Virginia NELAP 10490 06-14-20
Washington State C583-19 08-05-20
Washington State Program C583 08-03-20
West Virginia DEP State Program 354 11-30-19
Wisconsin State 999615430 08-31-20
Wisconsin State Program 999615430 08-31-20
Wyoming (UST) A2LA 2907.01 10-31-19
Eurofins TestAmerica, Denver
Page 48 of 54 Page 94 <9@tl2019
"'O Q)
(C
CD
~ <O
0 -01 ~
"C a, cc CD
<O 01
Q:,
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Ener2r Laboratories, Inc.
2393 Salt Creek Hwy
Casper. WY 82601-960 I
307.235.0515
Subcontractor:
Test America
4955 Yarrow St
Arvada. CO 80002
TEL: [phone]
FAX:
Acct #: 3037360100
Subcontractor's Client
C19081073-001C
C19081073-001 D
C19081073-001F
Aaueous
Aaueous
Aaueous
1m~liHi!~IIIH~im111~1111
C19081073
PO: ______ _
08/21/19 08:35 A I 1 -250ML-P-F-HN03
CHAIN-OF-CUSTODY RECORD
Earliest HT Expires: Wed, 8/28/2019 0835
Test Codes: SVOC-3SIOC-8270 Earliest Due Date:
Page 1 of 3
23-Aug-19
9/27/2019
# Bus. Days Until Due: 24
ReQuested Tests
C) "ll en CJ) < ~ :II < < 0 "ll 0 0 ()
:::r:: C) c;, cio :r: 'il (,) 00 "' Gl u, "' a,
"' "' 0 ...., ~ .... '? .... ~ C) ~ :r: u, cio ~ ,,
"' ~ ....,
Cl 0
-->---------------1 1 -...._ ...._ --.._ -----.._ .._ ---------------··-·-DD OJ OJ DD DD DD DD DD DD 08/21/19 08:35 A !2-1L-AG-NM-UP
------------------DDDDOJDDDDDDDDDDD 08/21/19 08:35 A 13 -40ML-CG-VOA-HCL
C 19081073-002C Aqueous 08/21/19 09:05 A I 1 -250ML-P-F-HN03 _. __ ~ __ _.OJOJDDDDDDDDDDDDDD
C19081073-002D
C19081073-002F
C19081073-003C
C 19081073-003D
C 19081073-003F
Comments:
QC Level:
11E(2)
Aaueous
Aaueous
Aaueous
Aaueous
Aaueous
08/21/19 09:05 A I2-1L-AG-NM-UP --------------------DDITJITJDDDDDDDDDDDD
08/21/1909:05A 13-40ML-CG-VOA-HCL
08121/19 09:20 A I 1 -250ML-P-F-HN03
08/21/19 09:20 A {2 -1L-AG-NM-UP
08/21/19 09:20 A 13 -40ML-CG-VOA-HCL
I -----------1----------IDDDDITJDDDDDDDDDDD
1----------1----------IOJOJDDDDDDDDDDDDDD
I ---------1------I D D OJ ITl D D D D D D D D D D D D
I -------1---------IDDDDITlDDDClnDDDDOD
280-127755 Chain of Custody ---
~8C/9':57
Date/Time9-
Relinquished by: {-~~:d 4r(yL ~?% f?'-18' ,
Relinquished by: .,. ~d';_ t' 2/ .5 0
Received by: r-~ ,(:::::::-,.,,, ;> <(/z'"t/1C, ~
Received by: I otf S
Shipped By: \.._) '?S Intact
G)N Receipt Temp: ""2. .4:i"17_&,12-S ·c
~
Temp Blank
v 0 N
"U Dl (C
CD
01 0
0 -01 .i:,..
"'tl Q) co CD
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0)
a,
~
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Enerior Laboratories, Inc.
2393 Salt Creek Hwy
Casper, WY 82601-960 I
307,235.051 S
Subcontractor:
Test America
4955 Yarrow St
Arvada. CO 80002
TEL: [phone]
FAX:
Acct#: 3037360100
Subcontractor's Client
C 19081073-004C
C19081073-004D
C19081073-004F
C 19081073-00SC
C 19081073-00SD
C 19081073-00SF
C19081073-006C
C19081073-006D
C19081073-006F
Comments:
QC Level: I
11E(2)
Aaueous
AQueous
AQueous
Aaueous
Aaueous
Aaueous
Aaueous
Aaueous
Aaueous
PO:.~~~~~~~
08/21/19 09:40 A I 1 -250ML-P-F-HN03
CHAIN-Of-CUSTODY RECORD
Earliest HT Expires: Wed, 8/28/2019 0835
Test Codes: SVOC-3510C-8270 Earliest Due Date:
Page 2 of3
23-Aug-19
9/27/2015
# Bus. Days Until Due: 24
Reauested Tests
(") "1l en en c§ ~ ::a < < "1l 0 0 (") ± (") (") cio ::i: G) w 00 "' G) N) U1 I\) 0,
0 .... 0 I\) .r:,. '? .!,t .r:,. ~ (") ~ ::i: U1 ..... 00 * "Tl l\l :E ....
Cl 0
----~ ----,__ --,__ ---1 1 ---------------------------------DDOJl:2JDDDDDDDDDDDD 08/21/19 09:40 A 12 -1L-AG-NM-UP
08/21/19 09:40 A }3 -40ML-CG-VOA-HCL --~--~DDDDOJDDDDDDDDDDD
08/21/19 09:45 A I 1 -250ML-P-F-HN03 --~--~OJOJDDDDDDDDDDDDDD
08/21/19 09:45 A J 2 -1 L-AG-NM-UP ------------------DDIJJIJJDDDDDDDDDDDD
08/21/19 09:45A J3-40ML-CG-VOA-HCL ------------DDDDOJDDDDDDDDDDD
08/21/1910:15 A 11 -250ML-P-F-HN03 ___________ OJOJDDDDDDDDDDDDDD
-----------D D CD CD D D D D D D D D D D D D 08/21/1910:15 A }2 -1L-AG-NM-UP
08/21/1910:15A f3-40ML-CG-VOA-HCL L----~DDDDOJDDDDDDDDDDD
/f-~;ed ,;) B-t?/9 57 g-
/, ~ D,t.rfim,
RelinqW,h,d by,t-~ i,peAA«-< ,4_ ~-. ,"/',I Ii
Relinquished by: ---2-,r,~'7' 2 Yo
Re"Wod by, ~ :::=::,
Received by:---------------
~~/Time . 'Ii JC> "/5"
Shipped By: 00 Custody Seal
~N Receipt Temp· '2~, 7.&,7-f . ·c
Intact
0N
Temp Blank
y G) On Ice
c:b N
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(l)
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Ener2}' Laboratories, Inc.
2393 Salt Creek Hwy
Casper, WY 82601-960 I
307.235.0515
Subcontractor:
Test America
4955 Yarrow St
Arvada. CO 80002
TEL: [phone]
FAX:
Acct#: 3037360100
Subcontractor's Client
C19081073-007C I
C 19081073-0070 I
C19081073-007F I
C19081073-008C I
C19081073-008D I
C19081073-008F I
Comments:
Aaueous
Aaueous
Aaueous
Aaueous
Aaueous
Aaueous
PO: ______ _
I OBf.21/1910:30 A !1 -250ML-P-F-HN03
CHAIN-OF-CUSTODY RECORD Page 3 of3
23-Aug-19
Earliest HT Expires: Wed, 8/28/2019 0835
Test Codes: SVOC-3510C-8270 Earliest Due Date:
#Bus.Days Until Due:
9/27/2019
24
Requested Tes1s
n -0 en en < < ::0 < < 0 ~ "'Cl 0 0 ~ :c c;, n
J: G> (.,) 00 "" G> ,(, u, I\) C)
,(, 0 -..J 0 ~ 0 !-t ~ ~ () ~ J: u, .... 00 * ,,
I\) ~ -.J
0 0
1--1--1--.__ ..._ .__ -t--1--1---,__ '-,__ I-1--
1 1 ,__ .__ ,__ ---,__ ,__ '--..__ ..__ ,__ .._ ,__ 1--1--.__ -----------···---DDOJDJDDDDDDDDDDDD I 08/21/1910:30 A 12 -1L-AG-NM-UP
I 08/21/1910:30 A 13 -40ML-CG-VOA-HCL -------------------DDDDOJDDDDDDDDDDD
I 08/21/19 08:35 A I 1 -250ML-P-F-HN03 ------------,----·-·. -·---.OJOJDDDDDDDDDDDDDD
I 08/21/19 08:35 A f 2 -1L-AG-NM-UP ------~DDffiffiDDDDDDDDDDDD
I 08/21/19 08:35 A J3 -40ML-CG-VOA-HCL L-----~-DDD DOJDDDDDDDDDDD
QC Level:
11E(2) P~./ee-:r ;} s ()/ c; :.i 7~ ~--...
Shipped By: \ )0 Cystody Seal I J_~~act ~N (i,N
~ <{/,°;Jf::~
Receipt Temp: 0 . S ), (p1 Z$ r , ·c
~
TempB~k
y (_r)v"
~Ice
u) N
Login Sample Receipt Checklist
Client: Energy Laboratories, Inc.
Login Number: 127755
List Number: 1
Creator: Petunln, Peter
Question Answer
Job Number: 280-127755-1
List Source: Eurofins TestAmerica, Denver
Comment -------------------------------Radioactivity wasn't checked or is </= background as measured by a survey True
meter.
The cooler's custody seal, if present, is intact. True
Sample custody seals, if present, are intact. True
The cooler or samples do not appear to have been compromised or True
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
True
False
True
True
True
True
True
There are no discrepancies between the containers received and the COC. False
Samples are received within Holding Time (excluding tests with immediate True
HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. NIA
Eurofins TestAmerica, Denver
Page 54 of 54
Cooler temperature outside required temperature
criteria.
Refer to Job Narrative for details.
Page 1 DO of9®:1./2019
······-·-····· LINKS ........... .
,
Revi~w your project
results through
Totci Accr:s:,
.;~ eurofins Environment Testing
TestAmerica
ANALYTICAL REPORT
Eurofins TestAmerica, Denver
4955 Yarrow Street
Arvada, CO 80002
Tel: [phone]
Laboratory Job ID: 280-127755-2
Client Project/Site: 11 (e) Byproduct Material
For:
Energy Laboratories, Inc.
2393 North Salt Creek Highway
PO BOX 247
Casper, Wyoming 82601
Attn: Ms. Tessa Parke
Authorized for release by:
10/30/2019 1:58:52 PM
Ivan Vania, Project Manager 11
(314 )298-8566
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TN/ requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
Page 101 of 172
I
Client: Energy Laboratories, Inc.
ProjecUSite: 11(e) Byproduct Material
Laboratory Job ID: 280-127755-2 I
Table of Contents
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
Chronicle. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Receipt Checklists ......................................... 24
Page 2 of 25 Page 102 of 172
I
Client: Energy Laboratories, Inc.
ProjecUSite: 11 (e) Byproduct Material
Qualifiers
Metals
Qualifier Qualifier Description
Definitions/Glossary
Job ID: 280-127755-2
j
Glossary
Abbreviation
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
a
%R
CFL
CNF
DER
Oil Fae
DL
DL, RA, RE, IN
DLC
EDL
LOO
LOQ
MDA
MDC
MDL
ML
NC
ND
PQL
QC
RER
RL
RPO
TEF
TEQ
These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis
Percent Recovery
Contains Free Liquid
Contains No Free Liquid
Duplicate Error Ratio (normalized absolute difference)
Dilution Factor
Detection Limit (DoD/DOE)
Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
Decision Level Concentration (Radiochemistry)
Estimated Detection Limit (Dioxin)
Limit of Detection (DoD/DOE)
Limit of Quantitation (DoD/DOE)
Minimum Detectable Activity (Radiochemistry)
Minimum Detectable Concentration (Radiochemistry)
Method Detection Limit
Minimum Level (Dioxin)
Not Calculated
Not Detected at the reporting limit (or MDL or EDL if shown)
Practical Quantitation Limit
Quality Control
Relative Error Ratio (Radiochemistry)
Reporting Limit or Requested Limit (Radiochemistry)
Relative Percent Difference, a measure of the relative difference between two points
Toxicity Equivalent Factor (Dioxin)
Toxicity Equivalent Quotient (Dioxin)
Page 3 of 25
Eurofins TestAmerica, Denver
Page 103 of 172
I
Client: Energy Laboratories, Inc.
Project/Site: 11 ( e) Byproduct Material
Job ID: 280-127755-2
Case Narrative
Laboratory: Eurofins TestAmerica, Denver
Narrative
CASE NARRATIVE
Client: Energy Laboratories, Inc.
Project: 11 (e) Byproduct Material
Report Number: 280-127755-2
Job ID: 280-127755-2
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 8/28/2019 10:45 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperatures of the 3 coolers at receipt time were 2.5° C, 2.8° C and 7.6° C.
Receipt Exceptions
The following sample was received by the laboratory; however, it was not listed on the Chain-of-Custody (COG): M3-54865
(280-127755-25). The sample was logged per the information stated on the sample container.
The following samples were received at the laboratory outside the required temperature criteria: C19081073-005D (280-127755-14),
C19081073-006D (280-127755-17), C19081073-007D (280-127755-20), and C19081073-008D (280-127755-23).
DISSOLVED METALS (ICP/MS)
Samples C19081073-001C (280-127755-1), C19081073-002C (280-127755-4), C19081073-003C (280-127755-7), C19081073-004C
(280-127755-10), C19081073-005C (280-127755-13), C19081073-006C (280-127755-16), C19081073-007C (280-127755-19),
C19081073-008C (280-127755-22) and M3-54865 (280-127755-25) were analyzed for Dissolved Metals (ICP/MS) in accordance with
200.8. The samples were prepared on 10/24/2019 and analyzed on 10/26/2019 and 10/29/2019.
Preparation Batch 160-447588, Analytical Batch 160-447983:
The serial dilution was outside control limits for Calcium indicating a potential matrix interference. : (240-119832-R-1-C SD)
The MS/MSD/serial dilution was analyzed on a different job within the preparation batch. The sample chosen for batch QC had a different
analyte list and QC requirements. As a result, the MS/MSD/serial dilution for Arsenic, Cobalt, Copper, Iron, Manganese, Molybdenum,
Nickel, Selenium, and Zinc was not applied to this job. Method performance is demonstrated by acceptable LCS recovery:
(240-119832-R-1-D MS), (240-119832-R-1-E MSD), and (240-119832-R-1-C SD).
The following samples were diluted to bring the concentration of target analytes within the calibration range. Elevated reporting limits
(Rls) are provided: C19081073-002C (280-127755-4), C19081073-003C (280-127755-7), C19081073-004C (280-127755-10),
C19081073-005C (280-127755-13), C19081073-006C (280-127755-16), C19081073-007C (280-127755-19), and C19081073-008C
(280-127755-22).
Preparation Batch 160-447588, Analytical Batch 160-448112:
Due to insufficient sample volume a dilution was performed for the following samples: C19081073-001 C (280-127755-1),
Page 4 of 25
Eurofins TestAmerica, Denver
Page 104 of 172
I
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Job ID: 280-127755-2 f Continued)
Case Narrative
Laboratory: Eurofins TestAmerica, Denver (Continued)
Job ID: 280-127755-2
C19081073-005C (280-127755-13), C19081073-006C (280-127755-16), C19081073-007C (280-127755-19), and C19081073-008C
(280-127755-22).
The following samples were diluted to bring the concentration of target analytes within the calibration range. In addition, the samples
caused internal standard failure when analyzed at a lesser dilution. Elevated reporting limits (Rls) are provided: C19081073-001C
(280-127755-1), C19081073-002C (280-127755-4), C19081073-003C (280-127755-7), C19081073-004C (280-127755-10),
C19081073-005C (280-127755-13), C19081073-006C (280-127755-16), C19081073-007C (280-127755-19), and C19081073-008C
(280-127755-22).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Page 5 of25
Eurofins TestAmerica, Denver
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I
I
Client: Energy Laboratories, Inc.
ProjecUSite: 11 (e) Byproduct Material
Method
200.8
200.7/200.8
Method Description
ICPMS Dissolved Metals by 200.8
Preparation, Metals
Protocol References:
EPA= US Environmental Protection Agency
Laboratory References:
Method Summary
TAL SL= Eurofins TestAmerica, St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Page 6 of 25
Protocol
EPA
EPA
Job ID: 280-127755-2
Laboratory
TAL SL
TAL SL
Eurofins TestAmerica, Denver
Page 106 of 172
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Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Lab Sample ID Client Sample ID
280-127755-1 C19081073-001C
280-127755-4 C 19081073-002C
280-127755-7 C 19081073-003C
280-127755-10 C 19081073-004C
280-127755-13 C 19081073-005C
280-127755-16 C 19081073-006C
280-127755-19 C 19081 073-007C
280-127755-22 C 19081073-008C
280-127755-25 M3-54865
Sample Summary
Job ID: 280-127755-2
Matrix Collected Received Asset ID
Water 08/21 /19 08:35 08/28/19 10:45
Water 08/21/19 09:05 08/28/19 10:45
Water 08/21/19 09:20 08/28/19 10:45
Water 08/21/19 09:40 08/28/19 10:45
Water 08/21/19 09:45 08/28/19 10:45 I Water 08/21/19 10:15 08/28/1910:45
Water 08/21/19 10:30 08/28/19 1 0:45
Water 08/21/19 08:35 08/28/19 10:45
Water 08/23/19 11 :20 08/28/19 10:45
Eurofins TestAmerica, Denver
Page 7 of 25 Page 107 of 172
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
Project/Site: 11(e) Byproduct Material
Method: 200.8 -ICPMS Dissolved Metals by 200.8 -Dissolved
Client Sample ID: C19081073-001C Lab Sample ID: 280-127755-1
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Arsenic 270 3.7 1.5 mg/L 10/24/19 13:54 10/29/1901 :25 500
Beryllium 0.93 0.18 0.074 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Cadmium 5.4 0.18 0.074 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Calcium 720 74 35 mg/L 10/24/19 13:54 10/29/1901 :25 500 I Chromium 15 3.7 1.5 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Cobalt 66 0.74 0.33 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Copper 1700 1.1 0.70 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Iron 9100 18 7.4 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Lead 22 1.1 0.37 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Magnesium 9200 18 7.4 mg/L 10/24/19 13:54 10/29/19 01:25 500
Manganese 540 1.5 0.55 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Molybdenum 120 1.8 0.74 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Nickel 110 1.8 0.74 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Potassium 2600 37 17 mg/L 10/24/19 13:54 10/29/1901 :25 500
Selenium 10 1.8 0.74 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Silver 0.79 0.74 0.33 mg/L 10/24/19 13:54 10/29/1901 :25 500
Sodium 28000 37 18 mg/L 10/24/19 13:54 10/29/1901 :25 500
Thallium ND 0.74 0.33 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Uranium 81 0.37 0.15 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Vanadium 1400 3.7 1.5 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Zinc 550 7.4 2.8 mg/L 10/24/19 13:54 10/29/1901 :25 500
Client Sample ID: C19081073-002C Lab Sample ID: 280-127755-4
Date Collected: 08/21/19 09:05 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Arsenic 23 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:24 ~
Beryllium 0.28 0.013 0.0050 mg/L 10/24/19 13:54 10/26/19 06:24 50
Cadmium 6.5 0.013 0.0050 mg/L 10/24/19 13:54 10/26/19 06:24 50
Calcium 480 5.0 2.4 mg/L 10/24/19 13:54 10/26/19 06:24 50
Chromium 2.1 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:24 50
Cobalt 54 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:24 50
Copper 160 0.75 0.48 mg/L 10/24/19 13:54 10/29/19 01 :31 500
Iron 3600 1.3 0.50 mg/L 10/24/19 13:54 10/26/19 06:24 50
Lead 0.59 0.075 0.025 mg/L 10/24/19 13:54 10/26/19 06:24 50
Magnesium 3700 1.3 0.50 mg/L 10/24/19 13:54 10/26/19 06:24 50
Manganese 170 0.10 0.038 mg/L 10/24/19 13:54 10/26/19 06:24 50
Molybdenum 3.2 0.13 0.050 mg/L 10/24/19 13:54 10/26/19 06:24 50
Nickel 140 1.3 0.50 mg/L 10/24/19 13:54 10/29/19 01:31 500
Potassium 710 2.5 1.1 mg/L 10/24/19 13:54 10/26/19 06:24 50
Selenium 1.3 0.13 0.050 mg/L 10/24/19 13:54 10/26/19 06:24 50
Silver ND 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:24 50
Sodium 4600 2.5 1.3 mg/L 10/24/19 13:54 10/26/19 06:24 50
Thallium 0.39 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:24 50
Uranium 29 0.025 0.010 mg/L 10/24/19 13:54 10/26/19 06:24 50
Vanadium 500 2.5 1.0 mg/L 10/24/19 13:54 10/29/19 01 :31 500
Zinc 850 5.0 1.9 mg/L 10/24/19 13:54 10/29/19 01:31 500
Eurofins TestAmerica, Denver
Page 8 of 25 Page 108 of 172
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
ProjecUSite: 11 (e) Byproduct Material
Method: 200.8 -ICPMS Dissolved Metals by 200.8 -Dissolved
Client Sample ID: C19081073-003C Lab Sample ID: 280-127755-7
Date Collected: 08/21/19 09:20 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Arsenic 0.38 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:31 --go
Beryllium 0.35 0.13 0.050 mg/L 10/24/19 13:54 10/29/19 01:38 500
Cadmium 7.4 0.013 0.0050 mg/L 10/24/19 13:54 10/26/19 06:31 50
Calcium 510 5.0 2.4 mg/L 10/24/19 13:54 10/26/19 06:31 50 I Chromium 0.23 J 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:31 50
Cobalt 64 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:31 50
Copper 35 0.075 0.048 mg/L 10/24/19 13:54 10/26/19 06:31 50
Iron 2500 1.3 0.50 mg/L 10/24/19 13:54 10/26/19 06:31 50
Lead ND 0.075 0.025 mg/L 10/24/19 13:54 10/26/19 06:31 50
Magnesium 10000 13 5.0 mg/L 10/24/19 13:54 10/2 9/ 1 9 01:38 500
Manganese 1000 1.0 0.38 mg/L 10/24/19 13:54 10/29/1901 :38 500
Molybdenum 0.55 0.13 0.050 mg/L 10/24/19 13:54 10/26/19 06:31 50
Nickel 150 1.3 0.50 mg/L 10/24/1913:54 10/29/19 01 :38 500
Potassium 630 2.5 1.1 mg/L 10/24/19 13:54 10/26/19 06:31 50
Selenium 2.9 0.13 0.050 mg/L 10/24/19 13:54 10/26/19 06:31 50
Silver 0.11 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:31 50
Sodium 14000 25 13 mg/L 10/24/19 13:54 10/29/19 01:38 500
Thallium 0.17 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:31 50
Uranium 19 0.025 0.010 mg/L 10/24/19 13:54 10/26/19 06:31 50
Vanadium 54 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:31 50
Zinc 950 5.0 1.9 mg/L 10/24/19 13:54 10/29/19 01:38 500
Client Sample ID: C19081073-004C Lab Sample ID: 280-127755-10
Date Collected: 08/21/19 09:40 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Arsenic 63 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:37 50
Beryllium 0.42 0.013 0.0050 mg/L 10/24/19 13:54 10/26/19 06:37 50
Cadmium 2.5 0.013 0.0050 mg/L 10/24/19 13:54 10/26/19 06:37 50
Calcium 510 50 24 mg/L 10/24/19 13:54 10/29/19 01 :45 500
Chromium 7.2 2.5 1.0 mg/L 10/24/19 13:54 10/29/1901 :45 500
Cobalt 28 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:37 50
Copper 580 0.75 0.48 mg/L 10/24/19 13:54 10/29/19 01:45 500
Iron 3200 1.3 0.50 mg/L 10/24/19 13:54 10126/19 06:37 50
Lead 9.0 0.075 0.025 mg/L 10/24/19 13:54 10/26/19 06:37 50
Magnesium 4100 13 5.0 mg/L 10124/19 13:54 10129/19 01 :45 500
Manganese 210 0.10 0.038 mg/L 10124119 13:54 10126119 06:37 50
Molybdenum 19 0.13 0.050 mg/L 10124119 13:54 10126/19 06:37 50
Nickel 50 0.13 0.050 mg/L 10124119 13:54 10126119 06:37 50
Potassium 1200 25 11 mg/L 10/24/19 13:54 10129/19 01 :45 500
Selenium 3.7 0.13 0.050 mg/L 10/24119 13:54 10/26119 06:37 50
Silver 0.31 0.050 0.023 mg/L 10124119 13:54 10126119 06:37 50
Sodium 15000 25 13 mg/L 10124119 13:54 10129119 01 :45 500
Thallium 0.090 0.050 0.023 mg/L 10124/19 13:54 10126119 06:37 50
Uranium 35 0.025 0.010 mg/L 10124/19 13:54 10/26/19 06:37 50
Vanadium 150 2.5 1.0 mg/L 10/24/19 13:54 10/29119 01 :45 500
Zinc 280 5.0 1.9 mg/L 10124119 13:54 10129119 01 :45 500
Eurofins TestAmerica, Denver
Page 9 of 25 Page 109 of 172
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
ProjecUSite: 11(e) Byproduct Material
Method: 200.8 -ICPMS Dissolved Metals by 200.8 -Dissolved
Client Sample ID: C19081073-005C Lab Sample ID: 280-127755-13
Date Collected: 08/21 /19 09:45 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Arsenic 52 0.36 0.14 mg/L 10/24/19 13:54 10/26/19 06:44 ~
Beryllium 0.37 0.018 0.0071 mg/L 10/24/19 13:54 10/26/19 06:44 50
Cadmium 1.9 0.018 0.0071 mg/L 10/24/19 13:54 10/26/19 06:44 50
Calcium 520 71 34 mg/L 10/24/19 13:54 10/29/19 01 :51 500 I Chromium 6.5 3.6 1.4 mg/L 10/24/19 13:54 10/29/1901 :51 500
Cobalt 25 0.071 0.032 mg/L 10/24/19 13:54 10/26/19 06:44 50
Copper 500 1.1 0.68 mg/L 10/24/19 13:54 10/29/19 01 :51 500
Iron 2500 1.8 0.71 mg/L 10/24/19 13:54 10/26/19 06:44 50
Lead 4.2 0.11 0.036 mg/L 10/24/19 13:54 10/26/19 06:44 50
Magnesium 3800 18 7.1 mg/L 10/24/19 13:54 10/29/1901 :51 500
Manganese 190 0.14 0.054 mg/L 10/24/19 13:54 10/26/19 06:44 50
Molybdenum 8.4 0.18 0.071 mg/L 10/24/19 13:54 10/26/19 06:44 50
Nickel 46 0.18 0.071 mg/L 10/24/19 13:54 10/26/19 06:44 50
Potassium 1000 36 16 mg/L 10/24/19 13:54 10/29/19 01 :51 500
Selenium 3.1 0.18 0.071 mg/L 10/24/19 13:54 10/26/19 06:44 50
Silver 0.23 0.071 0.032 mg/L 10/24/1913:54 10/26/19 06:44 50
Sodium 13000 36 18 mg/L 10/24/1913:54 10/29/1901 :51 500
Thallium 0.055 J 0.071 0.032 mg/L 10/24/19 13:54 10/26/19 06:44 50
Uranium 38 0.036 0.014 mg/L 10/24/19 13:54 10/26/19 06:44 50
Vanadium 130 3.6 1.4 mg/L 10/24/19 13:54 10/29/1901 :51 500
Zinc 210 0.71 0.27 mg/L 10/24/19 13:54 10/26/19 06:44 50
Client Sample ID: C19081073-006C Lab Sample ID: 280-127755-16
Date Collected: 08/21 /19 10: 15 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Arsenic 140 0.50 0.20 mg/L 10/24/19 13:54 10/26/19 06:51 ~
Beryllium 0.64 0.025 0.010 mg/L 10/24/19 13:54 10/26/19 06:51 50
Cadmium 2.0 0.025 0.010 mg/L 10/24/19 13:54 10/26/19 06:51 50
Calcium 670 100 48 mg/L 10/24/19 13:54 10/29/19 01 :58 500
Chromium 12 5.0 2.0 mg/L 10/24/19 13:54 10/29/1901 :58 500
Cobalt 44 0.10 0.045 mg/L 10/24/19 13:54 10/26/19 06:51 50
Copper 830 1.5 0.95 mg/L 10/24/19 13:54 10/29/1901 :58 500
Iron 5800 2.5 1.0 mg/L 10/24/19 13:54 10/26/19 06:51 50
Lead 16 0.15 0.050 mg/L 10/24/19 13:54 10/26/19 06:51 50
Magnesium 6500 25 10 mg/L 10/24/19 13:54 10/29/19 01 :58 500
Manganese 320 0.20 0.075 mg/L 10/24/19 13:54 10/26/19 06:51 50
Molybdenum 29 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:51 50
Nickel 78 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:51 50
Potassium 1900 50 23 mg/L 10/24/19 13:54 10/29/1901 :58 500
Selenium 6.6 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:51 50
Silver 0.17 0.10 0.045 mg/L 10/24/19 13:54 10/26/19 06:51 50
Sodium 18000 50 25 mg/L 10/24/19 13:54 10/29/19 01 :58 500
Thallium ND 0.10 0.045 mg/L 10/24/19 13:54 10/26/19 06:51 50
Uranium 36 0.050 0.020 mg/L 10/24/19 13:54 10/26/19 06:51 50
Vanadium 710 5.0 2.0 mg/L 10/24/19 13:54 10/29/19 01 :58 500
Zinc 280 1.0 0.38 mg/L 10/24/19 13:54 10/26/19 06:51 50
Eurofins TestAmerica, Denver
Page 10 of 25 Page 110 of 172
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
Project/Site: 11 (e) Byproduct Material
Method: 200.8 -ICPMS Dissolved Metals by 200.8 -Dissolved
Client Sample ID: C19081073-007C Lab Sample ID: 280-127755-19
Date Collected: 08/21/19 10:30 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Arsenic 89 0.50 0.20 mg/L 10/24/19 13:54 10/26/19 06:58 50
Beryllium 0.47 0.025 0.010 mg/L 10/24/19 13:54 10/26/19 06:58 50
Cadmium 2.0 0.025 0.010 mg/L 10/24/19 13:54 10/26/19 06:58 50
Calcium 550 100 48 mg/L 10/24/19 13:54 10/29/19 02:05 500 I Chromium 9.1 5.0 2.0 mg/L 10/24/19 13:54 10/29/19 02:05 500
Cobalt 31 0.10 0.045 mg/L 10/24/19 13:54 10/26/19 06:58 50
Copper 550 1.5 0.95 mg/L 10/24/19 13:54 10/29/19 02:05 500
Iron 4400 2.5 1.0 mg/L 10/24/19 13:54 10/26/19 06:58 50
Lead 7.8 0.15 0.050 mg/L 10/24/19 13:54 10/26/19 06:58 50
Magnesium 4800 25 10 mg/L 10/24/19 13:54 10/29/19 02:05 500
Manganese 240 0.20 0.075 mg/L 10/24/19 13:54 10/26/19 06:58 50
Molybdenum 27 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:58 50
Nickel 59 0.25 0.10 mg/L 10/24/1913:54 10/26/19 06:58 50
Potassium 1400 50 23 mg/L 10/24/19 13:54 10/29/19 02:05 500
Selenium 4.7 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:58 50
Silver 0.17 0.10 0.045 mg/L 10/24/19 13:54 10/26/19 06:58 50
Sodium 13000 50 25 mg/L 10/24/19 13:54 10/29/19 02:05 500
Thallium 0.087 J 0.10 0.045 mg/L 10/24/19 13:54 10/26/19 06:58 50
Uranium 31 0.050 0.020 mg/L 10/24/19 13:54 10/26/19 06:58 50
Vanadium 760 5.0 2.0 mg/L 10/24/19 13:54 10/29/19 02:05 500
Zinc 280 1.0 0.38 mg/L 10/24/19 13:54 10/26/19 06:58 50
Client Sample ID: C19081073-008C Lab Sample ID: 280-127755-22
Date Collected: 08/21/19 08:35 Matrix: Water
1 Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Arsenic 230 ---1.-3 0.50 mg/L 10/24/19 13:54 10/26/19 07:25 -~50
Beryllium 0.90 0.063 0.025 mg/L 10/24/19 13:54 10/26/19 07:25 50
Cadmium 4.8 0.063 0.025 mg/L 10/24/19 13:54 10126/19 07:25 50
Calcium 620 25 12 mg/L 10/24/19 13:54 10/26/19 07:25 50
Chromium 12 1.3 0.50 mg/L 10/24/19 13:54 10/26/19 07:25 50
Cobalt 60 0.25 0.11 mg/L 10/24/19 13:54 10/26/19 07:25 50
Copper 1500 3.8 2.4 mg/L 10/24/19 13:54 10/29/19 02:12 500
Iron 7800 6.3 2.5 mg/L 10/24/19 13:54 10/26/19 07:25 50
Lead 22 0.38 0.13 mg/L 10/24/19 13:54 10/26/19 07:25 50
Magnesium 7000 6.3 2.5 mg/L 10/24/19 13:54 10/26/19 07:25 50
Manganese 470 0.50 0.19 mg/L 10/24/19 13:54 10/26/19 07:25 50
Molybdenum 110 0.63 0.25 mg/L 10/24/19 13:54 10/26/19 07:25 50
Nickel 90 0.63 0.25 mg/L 10/24/19 13:54 10/26/19 07:25 50
Potassium 1900 13 5.6 mg/L 10/24/19 13:54 10/26/19 07:25 50
Selenium 7.9 0.63 0.25 mg/L 10/24/19 13:54 10/26/19 07:25 50
Silver 0.69 0.25 0.11 mg/L 10/24/19 13:54 10/26/19 07:25 50
Sodium 21000 13 6.3 mg/L 10/24/19 13:54 10/26/19 07:25 50
Thallium 0.13 J 0.25 0.11 mg/L 10/24/19 13:54 10/26/19 07:25 50
Uranium 77 0.13 0.050 mg/L 10/24/19 13:54 10/26/19 07:25 50
Vanadium 1300 13 5.0 mg/L 10/24/19 13:54 10/29/19 02: 12 500
Zinc 490 2.5 0.94 mg/L 10/24/19 13:54 10/26/19 07:25 50
Eurofins TestAmerica, Denver
Page 11 of 25 Page 111 of 172
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
ProjecUSite: 11 (e) Byproduct Material
Method: 200.8 -ICPMS Dissolved Metals by 200.8 -Dissolved
Client Sample ID: M3-54865 Lab Sample ID: 280-127755-25
Date Collected: 08/23/19 11 : 20 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Arsenic ND 0.010 0.0040 mg/L 10/24/19 13:54 10/29/19 02:18 ---2
Beryllium ND 0.00050 0.00020 mg/L 10/24/19 13:54 10/29/19 02:18 2
Cadmium ND 0.00050 0.00020 mg/L 10/24/19 13:54 10/29/19 02:18 2
Calcium 0.22 0.20 0.096 mg/L 10/24/19 13:54 10/29/19 02:18 2 I Chromium ND 0.010 0.0040 mg/L 10/24/19 13:54 10/29/19 02:18 2
Cobalt 0.0011 J 0.0020 0.00090 mg/L 10/24/19 13:54 10/29/19 02:18 2
Copper 0.021 0.0030 0.0019 mg/L 10/24/19 13:54 10/29/19 02:18 2
Iron 0.12 0.050 0.020 mg/L 10/24/19 13:54 10/29/19 02:18 2
Lead ND 0.0030 0.0010 mg/L 10/24/19 13:54 10/29/19 02:18 2
Magnesium 0.18 0.050 0.020 mg/L 10/24/19 13:54 10/29/19 02:18 2
Manganese 0.0084 0.0040 0.0015 mg/L 10/24/19 13:54 10/29/19 02:18 2
Molybdenum ND 0.0050 0.0020 mg/L 10/24/19 13:54 10/29/19 02:18 2
Nickel 0.0022 J 0.0050 0.0020 mg/L 10/24/19 13:54 10/29/19 02:18 2
Potassium 0.048 J 0.10 0.045 mg/L 10/24/19 13:54 10/29/19 02:18 2
Selenium ND 0.0050 0.0020 mg/L 10/24/19 13:54 10/29/19 02:18 2
Silver ND 0.0020 0.00090 mg/L 10/24/19 13:54 10/29/19 02:18 2
Sodium 0.62 0.10 0.050 mg/L 10/24/19 13:54 10/29/19 02:18 2
Thallium ND 0.0020 0.00090 mg/L 10/24/19 13:54 10/29/19 02:18 2
Uranium 0.0015 0.0010 0.00040 mg/L 10/24/19 13:54 10/29/19 02:18 2
Vanadium 0.0063 J 0.010 0.0040 mg/L 10/24/19 13:54 10/29/19 02:18 2
Zinc 0.014 J 0.020 0.0075 mg/L 10/24/19 13:54 10/29/19 02:18 2
Eurofins TestAmerica, Denver
Page 12 of 25 Page 112 of 172
QC Sample Results
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Method: 200.8 -ICPMS Dissolved Metals by 200.8
Lab Sample ID: MB 160-447588/1-A
Matrix: Water
Analysis Batch: 447983
MB
Analyte Result
Arsenic
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Uranium
Vanadium
Zinc
Lab Sample ID: LCS 160-447588/2-A
Matrix: Water
Analysis Batch: 447983
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
MB
Qualifier RL
0.010
0.00050
0.00050
0.20
0.010
0.0020
0.0030
0.050
0.0030
0.050
0.0040
0.0050
0.0050
0.10
0.0050
0.0020
0.10
0.0020
0.0010
0.010
0.020
Spike
MOL
0.0040
0.00020
0.00020
0.096
0.0040
0.00090
0.0019
0.020
0.0010
0.020
0.0015
0.0020
0.0020
0.045
0.0020
0.00090
0.050
0.00090
0.00040
0.0040
0.0075
LCS LCS
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Analyte Added Result Qualifier
Arsenic
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Uranium
Vanadium
Zinc
1.00 0.970
0.100 0.0965
1.00 1.05
10.0 10.5
1.00 0.959
1.00 1.00
1.00 1.01
10.0 9.81
1.00 1.04
10.0 9.86
1.00 1.04
0.500 0.531
1.00 0.974
10.0 9.60
0.500 0.468
0.200 0.205
10.0 9.88
0.200 0.210
1.00 1.05
1.00 0.969
1.00 0.948
Page 13 of 25
Job ID: 280-127755-2
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 447588
D Prepared Analyzed Dil Fae
10/24/19 13:54 10/26/19 06:03 --2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2 I 10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 447588
%Rec.
Unit D %Rec Limits
mg/L ~ 85-115 ----
mg/L 96 85 -115
mg/L 105 85-115
mg/L 105 85-115
mg/L 96 85-115
mg/L 100 85-115
mg/L 101 85-115
mg/L 98 85-115
mg/L 104 85-115
mg/L 99 85-115
mg/L 104 85-115
mg/L 106 85-115
mg/L 97 85-115
mg/L 96 85-115
mg/L 94 85-115
mg/L 102 85-115
mg/L 99 85-115
mg/L 105 85-115
mg/L 105 85-115
mg/L 97 85-115
mg/L 95 85-115
Eurofins TestAmerica, Denver
Page 113 of 172
QC Association Summary
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
Project/Site: 11 (e) Byproduct Material
Metals
Prep Batch: 447588
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
280-127755-1 C19081073-001C Dissolved Water 200.7/200.8
280-127755-4 C 19081073-002C Dissolved Water 200.7/200.8
280-127755-7 C 19081073-003C Dissolved Water 200.7/200.8
280-127755-10 C19081073-004C Dissolved Water 200.7/200.8
280-127755-13 C 19081073-005C Dissolved Water 200.7/200.8
280-127755-16 C19081073-006C Dissolved Water 200.7/200.8
280-127755-19 C19081073-007C Dissolved Water 200.7/200.8
280-127755-22 C19081073-008C Dissolved Water 200.7/200.8
280-127755-25 M3-54865 Dissolved Water 200.7/200.8
MB 160-447588/1-A Method Blank Total/NA Water 200.7/200.8 I LCS 160-447588/2-A Lab Control Sample Total/NA Water 200.7/200.8
Analysis Batch: 447983
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
280-1277 55-4 C19081073-002C Dissolved Water 200.8 447588
280-1277 55-7 C19081073-003C Dissolved Water 200.8 447588
280-1277 55-10 C 19081073-004C Dissolved Water 200.8 447588
280-1277 55-13 C 19081073-005C Dissolved Water 200.8 447588
280-1277 55-16 C 19081073-006C Dissolved Water 200.8 447588
280-1277 55-19 C 19081073-007C Dissolved Water 200.8 447588
280-127755-22 C 19081073-008C Dissolved Water 200.8 447588
MB 160-447588/1-A Method Blank Total/NA Water 200.8 447588
LCS 160-447588/2-A Lab Control Sample Total/NA Water 200.8 447588
Analysis Batch: 448112
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
280-127755-1 C19081073-001C Dissolved Water 200.8 447588
280-127755-4 C 19081073-002C Dissolved Water 200.8 447588
280-127755-7 C 19081073-003C Dissolved Water 200.8 447588
280-127755-10 C19081073-004C Dissolved Water 200.8 447588
280-127755-13 C 19081073-005C Dissolved Water 200.8 447588
280-127755-16 C19081073-006C Dissolved Water 200.8 447588
280-127755-19 C19081073-007C Dissolved Water 200.8 447588
280-127755-22 C19081073-008C Dissolved Water 200.8 447588
280-127755-25 M3-54865 Dissolved Water 200.8 447588
Eurofins TestAmerica, Denver
Page 14 of 25 Page 114 of 172
Lab Chronicle
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
ProjecUSite: 11 (e) Byproduct Material
Client Sample ID: C19081073-001 C Lab Sample ID: 280-127755-1
Date Collected: 08/21 /19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab ----Dissolved Prep 200.7/200.8 34 ml 50 ml 447588 10/24/19 13:54 LAM TALSL
Dissolved Analysis 200.8 500 448112 10/29/1901 :25 FLC TALSL
Client Sample ID: C19081073-002C Lab Sample ID: 280-127755-4
Date Collected: 08/21/19 09:05 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 200.7/200.8 ~50ml 50 m---C--4475mr-10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 50 447983 10/26/19 06:24 FLC TAL SL
Dissolved Prep 200.7/200.8 50 ml 50 ml 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 500 448112 10/29/1901 :31 FLC TAL SL
Client Sample ID: C19081073-003C Lab Sample ID: 280-127755-7
Date Collected: 08/21/19 09:20 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab ----Dissolved Prep 200.7/200.8 50 ml 50 ml 447588 10/24/19 13:54 LAM TALSL
Dissolved Analysis 200.8 50 447983 10/26/19 06:31 FLC TALSL
Dissolved Prep 200.7/200.8 50 ml 50 ml 447588 10/24/19 13:54 LAM TALSL
Dissolved Analysis 200.8 500 448112 10/29/1901 :38 FLC TALSL
Client Sample ID: C19081073-004C Lab Sample ID: 280-127755-10
Date Collected: 08/21/19 09:40 Matrix: Water
Date Received: 08/28/1910:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab ----Dissolved Prep 200.7/200.8 50 ml 50 ml 447588 10/24/19 13:54 LAM TALSL
Dissolved Analysis 200.8 50 447983 10/26/19 06:37 FLC TALSL
Dissolved Prep 200.7/200.8 50 ml 50 ml 447588 10/24/19 13:54 LAM TALSL
Dissolved Analysis 200.8 500 448112 10/29/1901 :45 FLC TALSL
Client Sample ID: C19081073-005C Lab Sample ID: 280-127755-13
Date Collected: 08/21 /19 09:45 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab ----Dissolved Prep 200.7/200.8 35 ml 50 ml 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 50 447983 10/26/19 06:44 FLC TALSL
Dissolved Prep 200.7/200.8 35 ml 50 ml 447588 10/24/19 13:54 LAM TALSL
Dissolved Analysis 200.8 500 448112 10/29/19 01 :51 FLC TALSL
Eurofins TestAmerica, Denver
Page 15 of 25 Page 115 of 172
Lab Chronicle
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
Project/Site: 11 (e) Byproduct Material
Client Sample ID: C19081073-006C Lab Sample ID: 280-127755-16
Date Collected: 08/21/19 10:15 Matrix: Water
Date Received: 08/28/1910:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved ~ 200.7/200.8 25 ml 50 mL 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 50 447983 10/26119 06:51 FLC TAL SL
Dissolved Prep 200.7/200.8 25 mL 50 mL 447588 10124119 13:54 LAM TALSL
Dissolved Analysis 200.8 500 448112 10129/19 01 :58 FLC TALSL
Client Sample ID: C19081073-007C Lab Sample ID: 280-127755-19
Date Collected: 08/21/19 10:30 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared m Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab -----Dissolved Prep 200.71200.8 25 ml 50 ml 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 50 447983 10/26119 06:58 FLC TALSL
Dissolved Prep 200.7/200.8 25 ml 50 ml 447588 10/24119 13:54 LAM TAL SL
Dissolved Analysis 200.8 500 448112 10/29119 02:05 FLC TALSL
Client Sample ID: C19081073-008C Lab Sample ID: 280-127755-22
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 200.71200.8 10 ml 50 ml 447588 10/24/19 13:54 LAM TALSL
Dissolved Analysis 200.8 50 447983 10/26/19 07:25 FLC TAL SL
Dissolved Prep 200.7/200.8 10 ml 50 ml 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 500 448112 10/29119 02: 12 FLC TAL SL
Client Sample ID: M3-54865 Lab Sample ID: 280-127755-25
Date Collected: 08/23/19 11 : 20 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 200.7/200.8 50ml 50ml 447588 10/24/19 13:54 LAM TALSL
Dissolved Analysis 200.8 2 448112 10129/19 02:18 FLC TAL SL
Laboratory References:
TAL SL= Eurofins TestAmerica, St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins TestAmerica, Denver
Page 16 of 25 Page 116 of 172
Accreditation/Certification Summary
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Laboratory: Eurofins TestAmerica, Denver
Job ID: 280-127755-2
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
A2LA Dept. of Defense ELAP 2907.01 10-31-19
A2LA ISO/IEC 17025 2907.01 10-31-19
Alabama State Program 40730 09-30-12 *
Alaska (UST) State 18-001 01-08-20
Arizona State AZ0713 12-20-19
Arkansas DEQ State 19-047-0 06-01-20
California State 2513 01-08-20
Connecticut State PH-0686 09-30-20
Florida NELAP E87667-57 06-30-20
Georgia State 4025-011 01-08-20
Georgia State Program N/A 01-08-20
Illinois NELAP 2000172019-1 04-30-20
Iowa State IA#370 12-01-20
Kansas NELAP E-10166 04-30-20
Louisiana NELAP 30785 06-30-20
Maine State 2019011 [phone]
Maine State Program C00002 03-03-21
Minnesota NELAP 1545373 12-31-19
Nevada State C0000262020-1 07-31-20
New Hampshire NELAP 205310 04-28-20
New Hampshire NELAP 205319 04-28-20
New Jersey NELAP 190002 06-30-20
New York NELAP 59923 04-01-20
North Carolina (WW/SW) State <cert No.> 12-31-19
North Carolina (WW/SW) State Program 358 12-31-19
North Dakota State R-034 01-08-20
Oregon NELAP 4025-011 01-08-20
Pennsylvania NELAP 013 08-01-20
South Carolina State 72002001 01-08-20
South Carolina State Program 72002001 01-08-20
Texas NELAP T104704183-19-17 09-30-20
US Fish & Wildlife Federal 07-31-20
US Fish & Wildlife US Federal Programs 058448 07-31-20
USDA Federal 03-26-21
USDA US Federal Programs P330-18-00099 03-26-21
Utah NELAP C0000262019-11 07-31-20
Virginia NELAP 10490 06-14-20
Washington State C583-19 08-05-20
West Virginia DEP State 354 11-30-19
West Virginia DEP State Program 354 11-30-19
Wisconsin State 999615430 08-31-20
Wyoming (UST) A2LA 2907.01 10-31-19
Wyoming (UST) A2LA 2907.01 10-31-21
* Accreditation/Certification renewal pending -accreditation/certification considered valid.
Eurofins TestAmerica, Denver
Page 17 of 25 Page 117 of 172
Accreditation/Certification Summary
Client: Energy Laboratories, Inc.
ProjecUSite: 11 ( e) Byproduct Material
Laboratory: Eurofins TestAmerica, St. Louis
Job ID: 280-127755-2
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
.A.NAB Dept. of Defense ELAP L2305 04-06-22
ANAB Dept. of Energy L2305.01 04-06-22
ANAB ISO/IEC 17025 L2305 04-06-22
Arizona State AZ0813 12-08-19
California Los Angeles County Sanitation 10259 06-30-20
Districts
California State 2886 06-30-20
Connecticut State PH-0241 03-31-21
Florida NELAP E87689 06-30-20
HI -RadChem Recognition State n/a 06-30-20
Illinois NELAP 004553 11-30-19
Iowa State 373 09-17-20
Iowa State Program 373 12-01-20
Kansas NELAP E-10236 10-31-19 *
Kentucky (DW) State KY90125 12-31-19
Louisiana NELAP 04080 06-30-20
Louisiana (DW) State LA011 12-31-19
Maryland State 310 09-30-20
Ml -RadChem Recognition State 9005 06-30-20
Missouri State 780 06-30-22
Nevada State M0000542020-1 07-31-20
New Jersey NELAP M0002 06-30-20
New York NELAP 11616 04-01-20
North Dakota State R-207 06-30-20
NRC NRC 24-24817-01 12-31-22
Oklahoma State 9997 08-31-20
Pennsylvania NELAP 68-00540 02-28-20
South Carolina State 85002001 06-30-20
Texas NELAP T104704193-19-13 07-31-20
US Fish & Wildlife US Federal Programs 058448 07-31-20
USDA US Federal Programs P330-17-00028 02-02-20
Utah NELAP M0000542019-11 07-31-20
Virginia NELAP 10310 06-14-20
Washington State C592 08-30-20
Washington State Program C592 08-30-20
West Virginia DEP State 381 10-31-19
West Virginia DEP State Program 381 10-31-19 *
• Accreditation/Certification renewal pending -accreditation/certification considered valid.
Eurofins TestAmerica, Denver
Page 18 of 25 Page 118 of 172
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Energy Laboratories, Inc.
2393 Salt Creek Hwy
Casper, WY 82601-9601
307.235.0515
Subcontractor:
Test America
4955 Yarrow St
Arvada. CO 80002
TEL: [phone]
FAX:
Acct #: 3037360100
Subcontractor's Client
C19081073-001C
C19081073-001 D
AQueous
Aqueous
lilli!IIH~i~l~llmm111~1H
C19081073
PO: ______ _
08121/19 08:35 A ! 1 -250ML-P-F-HN03
CHAIN-OF-CUSTODY RECORD
Earliest HT Expires: Wed, 8/28/2019 0835
Test Codes: SVOC-35 I OC-8270 Earliest Due Date:
Page 1 of 3
23-Aug-19
9/27/2015
#Bus.Days Until Due: 24
Reauested Tests
C) -0 en ~ < < J) < 0 ~ -0 0 0 C) ± Q 0 ' &, 00 I '? w "' G'l (JI N 0,
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C19081073-002C
C 19081073-002D
C19081073-002F
C 19081073-003C
C19081073-003D
C19081073-003F
Comments:
QC Level:
11E(2)
Aaueoos
Aqueous
Aqueous
Aqueous
Aaueous
Aaueous
08/21/19 09:05 A J 1 -250ML-P-F-HN03 -----. ----. --ru ru DD DD DD DD DD DD DD
08121/19 09:0SA J2-1L-AG-NM-UP --·. ---·-----· DD ITI ITI DD DD DD DD DD DD
08/21/19 09:05 A 13 -40ML..CG-VOA-HCI ··---·--·,--··-,DDDDruDDDDDDDDDDD
08121119 09:20 A f 1 -250ML-P-F-HN03 I .. ------1----·-· lillruDDDDDDDDDDDDDD
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08/21/19 09:20 A f 3 -40ML-CG-VOA-HCL 1 1ooooruoooonoooooo
280-127755 Chain of Custody -----
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Relinquished by: ,~._;;.;.;.t)z;;; 7 ;!J'.5(
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2393 Salt Creek Hwy CHAIN-OF-CUSTODY RECORD Page 2 of 3
23-Aug-19
Casper, WY 82601-960 I
307.235.0515
Subcontractor.
Test America
4955 Yarrow St
Arvada. CO 80002
TEL: [phone]
FAX:
Acct#: 3037360100
Subcontractor's Client
C19081073-004C
C19081073-0040
C19081073-004F
C19081073-005C
C 19081073-0050
C19081073-005F
C19081073-006C
C 19081073-0060
C19081073-006F
Commeots:
QC Level:
11E(2)
PO: ______ _
Aaueous 08/21/19 09:40 A '1-250ML-P-F-HN03
Earliest HT Expires: Wed, 8/28/2019 0835
Test Codes: SVOC-3510C-8270 Earliest Due Date: 9/27/2015
# Bus. Days Until Due: 24
Reauested Tests
() "'O CJ) en < ~ ::0 < < 0 "'O 0 0 (") :c ~ (") 00 :x: G) &, N
G) ~ 01 "' 0,
0 ..... 0 ~ c;:, ~ !.II (") ~ (11 ~ co 71 * "' ..... ~ 0 0
-----~ ---------1--1 1 -..._ ---..._ ..._ --..._ ..._ --..._ -..._
Aaueous 08/21/19 09:40 A j2 -1 L-AG-NM-UP
Aaueous 08121/19 09:40 A 13 -40ML-CG-VOA-HCL
Aaueous 08121/19 09:45 A I1 -250ML-P-F-HN03
---·---·---·-----· DDIJJIJJDDDDDDDDDDDD
______ DDDD[!JDDDDDDDDDDD _________ IJJC!JDDDDDDDDDDDDDD
Aaueous 08121/19 09:45 A 12 -1L-AG-NM-UP ~-------DD[!J[!]00DDDDDDDDDD
Aaueous 08121/19 09:45 A 13 -40ML-CG-VOA-HCL ~-~-~~DDDD[!JDDDDDDDDDDD
Aaueous 08/21/1910:15A {1 -250ML-P-F-HN03 ~------mwDDDDDDDDDDDDDD
Aaueous
AQueous
08121/19 10:15 A J2 -1L-AG-NM-UP
08/21/1910:15 A 13 -40ML-CG-VOA-HCL
. -·-·····-oomwDDDDDDDDDDDD
____ ODDDC!JDDDDDDDDDDD
;} 8C>/9 5 7 8'
~~!Time . 'Ir 10 A/? Reeoiv,d by, ~ ::__::i
Received by: ---------------
Relioquished by:
Relinquished by:i-t-~""""'.,_ • ._=·'!:;.,...i,J,:,1=..:a"~'""c:::.,;'~'-""-..:.,J"::.:::-~c.'::::1~-";.;;;-::a...0=~-:.;."'""1~~,(,:L.,;t,4...~.......::...' .2.;w• ,:.._;_:l.::..:-0
Shipped By: uP Intact
N Receipt Temp· '2_~1 7.&17J( . ·c
~ -----1!'1
Temp Blank On Ice
y~ CT) N
"'O Q)
(C
CD
I\.) ......
0 -I\.) c.n
"'ll Ill <O (1) ....
I\) ....
s. ....
-..J I\)
Energy Laboratories, Inc.
2393 Salt Creek Hwy
Casper, WY 82601-960 l
307.235.0S IS
Subcontractor:
Test America
4955 Yarrow St
Arvada. CO 80002
TEL: [phone]
FAX:
Acct#: 3037360100
Subcontractor's Client
-I I C19081073--007C
C 19081073-0070
C19081073-007F
C19081073-008C
C19081073--008D
C19081073-00BF
Comments:
Aaueous
Aaueous
Aaueous
Aaueous
Aaueous
Aaueous
PO: ______ _
08/21/19 10:30 A ! 1 -250ML-P-F-HN03
08/21/19 10:30 A 12 -1L-AG-NM-UP
08/21/1910:30 A 13-40ML-CG-VOA-HCL
08/21/19 08:35 A I 1 -250ML-P-F-HN03
08/21/19 08:35 A !2 -1L-AG-NM-UP
08/21/19 08:35 A 13-40ML-CG-VOA-HCL
CHAIN-OF-CUSTODY RECORD Page 3 of3
23-Aug-19
Earliest HT Expires: Wed, 8/28/2019 0835
Test Codes: SVOC-35IOC-8270 Earliest Due Date:
#Bus.Days Until Due:
9/27/2019
24
ReQuested Tes1s
C') "Q {/I {/I < ~ ::0 < < 0 "Q 0 0 C') ::c C') C') QI> l, I ::i: G) C)O ..,
G) ;., en .., 0)
;., 0 ..... 0 "" 0 ~ "" !-71 (") ~ ::i: en .... 00 .,, ~ 1'J :E '-I 0 0
-t--t---~ --t--t----t-----t--
...!.. ..!... ----------------------------DDOJOJDDDDDDDDDDDD
DDDDOJDDDDDDDDDDD
OJOJDDDDDDDDDDOODD
DDOJOJDDDDDDDDDDDD
DDDDOJDDDDDDDDDDD
QC Level:
11E(2) p ,Vt'N ;) o {! I c; ::, 7 &--
Shipped By: \ )~
Cystody Seal I ~tact V N G_:. N
Dateffime ____/ ~ /z. g/ti Jot/5 -..,,..""----C-.------
Receipt Temp: .'.2-. '5, 7. '4:,, .zz C
11!!!1
TempB~~
y (jj,1'
Anlce
u) N
Energy Laboratories Inc Workorder Summary
Energy Fuels Resources (USA) Inc
Samp I Client Sample ID Collection Date Due Matrix Frac RT Done Test Code
T Analyte
C O O 200.7.8-W-D
11111111111 ~Ill llll 1111111111111111~ 111111111111
C19081073
Hold MS SEL Storage
MDL PQL MCL Units
D D 0 LG-2-000 ...................................................................................................................................................................................................
A Arsenic 0.0001 0.001 0 ug/L
A Beryllium 0.0001 0.001 0 ug/L
A Cadmium 0.00005 0.001 0 ug/L
A Calcium O.D3 0
A Chromium 0.0005 0.005 0 ug/L
A Cobalt 0.00005 0.005 0 ug/L
A Copper 0.0001 0.005 0 ug/L
A Iron 0.001 0.02 0 ug/L
A Lead 0.00005 0.001 0 ug/L
A Magnesium 0 05 1 0
A Manganese 0.00005 0.001 0 ug/L
A Molybdenum 0.00005 0.001 0 ug/L
A Nickel 0.0001 0.005 0 ug/L
A Potassium 0.0001 0
A Selenium 0.05 0.001 0 ug/L
A Sliver 0.4 0.001 0 ug/L
A Sodium 0.0001 1 0
A Thallium 0.0005 0.0005 0 ug/L
A Tin 0.0004 0.05 0 ug/L
A Uranium 0.00002 0.0003 0 ug/L
A Vanadium 0.0005 0.D1 0 ug/L
A Zinc 0.001 0. 0 u IL
Page 22 of 25 Page 122 of 172
"O D> cc
CD
N
(,)
0 -N
01
lJ ID (Cl (I)
~
l\l (..,)
a
.....
l\l
Eurofins TestAmerica, Denver
4955 Yarrow Street
Arvada. CO 80002
Phone: [phone] Fax: [phone]
Client Information {Sub Contract LabJ
Clienl Conlact:
Shipping/Receiving
Company:
ITestAmerica Laboratories. Inc.
Sa111p1er.
Phor>8'
Chain of Custody Record
lab PM;
Vania, Ivan H
E-Mail'
[e-mail]
!Accrl!<lttal,ons Required (See note):
IIIU~fflffiffilffllllillllll~l~ffi~~ ~~ eurofins
Carrier Tracking No(s):
Slate ol Origin:
Wyoming
COC No·
280-502172.1
Page:
Page 1 of 1
Job#:
280-127755-2
E:1vironrnt·;--;t icsti,.;.
1(:'-:;tAm~rr.;:;::t
Alldress: Due Date Requested: Preservation Codes:
13715 Rider Trail North. • 10/2812019 Analysis Requested A-HCL
City: TAT Requested (days): · B -NaOH
Earth City C -Zn Acelate
State. Zip: c O -Nitric Acid
MO 63045 w E -NaHS04 ' ~ F-MeOH
Phone: PO #: 5l G -Amchlor
314-298-8566(Tel) 314-298-8757(Fax) l'o !!! . z C Email: WO#: ... -oq
: i ~
Project Name: Pro1ect #'. i 15 o
11(e) Byproduct Material 28019578 :H I §l
H -Ascorbic Acid
I-Ice
I!! I J -DI Water :! K -EDTA !i L-EDA
g Other:
M· He~ane
N. None
O-AsNa02
P -Na204S
Q -Na2S03
R-Na25203
S -H2S04
T -TSP Dodecahydrate
u -Acetone
V -MCAA
W-pH4-5
Z -other (specify)
Stte: SSOWIJ: i i ~ .. "l!'!I __ ---
Sample Matrix ~ c' ... w
g ... .. it-_______ _j
Sample
Sample Identification -Client ID (Lab ID) Sample Date Time
·, -. -.. >< ...
08:35 C19081073-001C (280-127755-1) 8121/19 Mnunt:>in
C19081073-002C (280-127755-4) 8/21/19 09:05
Mountain
C19081073-003C (280-127755-7) 8/21/19 09:20
""""ntain
C19081073-004C (280-127755-10) 8/21/19 09:40
lAn,,nt~jn
C19081073-005C (280-127755-13) 8/21/19 09:45
Mn11nt:>in
C19081073-006C (280-127755-16) 8/21/19 10:15
Mountain
C19081073-007C (280-127755-19) 8/21/19 f0:30
Mnun•~;n
C19081073-00SC (280-127755-22) 8121/19 08:35
lAnuntain
M3-54865 (280-12n55-25) 8/23/19 11:20
Mount.fill
~
Type <--.•-i.11 (C=comp, o,w-.ion.
G=arab) e,-n..~ ..... .,,l
. Pri,se;vation ,Code:-· ~ ..... ~ ..........
Water
Water
Waler
Water
Water
Water
Water
Water
Water
!ii .,; 0 ...
X
X
X
X
X
X
X
X
X
§ z
J {:.
IX
1
Special Instructions/Note:
Note: Since laboratory accreditations are subject lo change. TestAmerica Laboratories. Inc places the ownership of method. analyte & accreditallon compliance upon out subcontract labo,alories, This sample shipment is forwarded under cha1n~f-<:ustody If the laboratory does not
currenUy maintain accreditabon in the Slate of Origin rosted abase for analysis/leslslmatrix being analyzed. lhe samples must be shipped baek to the Tes!America laboratory or other instructions v.ill be provided Any changes lo accreditation status shoukj be brought lo Tes!America
Laboratories, Inc. attention immediately. ~ all requested accreditations are currenl to date. return lhe signed Chain of Cuslody atteslmg to said complicance to TestAmerica Laboratories. Inc
Possible Hazard Identification
Level 1 radioactive
Deliverable Reciuested: I. II. Ill, N, Other (specify)
Empty Kit R!l)2ciu1shed by:
"-9 Re/inqulstled Dy. _
~
Rea~bY"-..;;;..___;;
Relinquished by:
Custody Seals lntao;L 'Custody Seal No.:
t. Yes t. No
Primary Deliverable Rank: 2
Date:
Di~?;~fr 1 '-/k
Oa1e11'ime: T
Datemme:
Sample Disposal ( A fee may be assessed if samples are retained longer than 1 monlh}
D Return To Client D Disposal By Lab D Archive For Months
Special Instructions/QC Requirements:
Time: Method or Shlpmenl:
Comi:oan}'. ,-.:~c..dr--?=< e'-11WtfL I O y:SS
Company _
7A5IL
Company Receised by: Dateffime; Company
Company Received by: Datemme: Company
Cooler Temperalure(s) "C and other Remarks.
Ver: 01/1612019
~
Login Sample Receipt Checklist
Client: Energy Laboratories, Inc.
Login Number: 127755
List Number: 1
Creator: Petunin, Peter
Question Answer
Radioactivity wasn't checked or is </= background as measured by a survey True
meter.
The cooler's custody seal, if present, is intact. True
Sample custody seals, if present, are intact. True
The cooler or samples do not appear to have been compromised or True
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no discrepancies between the containers received and the COC.
Samples are received within Holding Time (excluding tests with immediate
HTs)
True
False
True
True
True
True
True
False
True
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
Eurofins TestAmerica, Denver
Page 24 of 25
Job Number: 280-127755-2
List Source: Eurofins TestAmerica, Denver
Comment
Cooler temperature outside required temperature
criteria.
Refer to Job Narrative for details.
Page 124 of 172
Login Sample Receipt Checklist
Client: Energy Laboratories, Inc.
Login Number: 127755
List Number: 2
Creator: McKinney, Gerrod E
Question
Radioactivity wasn't checked or is </= background as measured by a survey
meter.
The cooler's custody seal, if present, is intact.
Sample custody seals, if present, are intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no discrepancies between the containers received and the COC.
Samples are received within Holding Time (excluding tests with immediate
HTs)
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Residual Chlorine Checked.
Eurofins TestAmerica, Denver
Answer
True
True
N/A
True
True
True
True
True
True
True
NIA
True
True
True
True
True
True
True
True
True
N/A
N/A
True
N/A
Page 25 of 25
Job Number: 280-127755-2
List Source: Eurofins TestAmerica, St. Louis
List Creation: 10/21/1901 :47 PM
Comment
Page 125 of 172
., ............ LINKS ........... .
r Review your project
results through
TotdAccess
ltlave a Question 7
~
k
The
Ex ert
Vlsit,us at:
www.testamericainc.com
_;~ eurofins Environment Testing
TestAmerica
ANALYTICAL REPORT
Eurofins TestAmerica, Denver
4955 Yarrow Street
Arvada, CO 80002
Tel: [phone]
Laboratory Job ID: 280-127755-2
Client Project/Site: 11 (e) Byproduct Material
Revision: 1
For:
Energy Laboratories, Inc.
2393 North Salt Creek Highway
PO BOX 247
Casper, Wyoming 82601
Attn: Ms. Tessa Parke
fa';f~
Authorized for release by:
11/25/2019 1:08:03 PM
Ivan Vania, Project Manager II
(314 )298-8566
ivan. [e-mail]
The test results in this report meet all 2003 NELAC and 2009 TN/ requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
Page 126 of 172
I
Client: Energy Laboratories, Inc.
Project/Site: 11(e) Byproduct Material
Table of Contents
Laboratory Job ID: 280-127755-2
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
Page 2 of 31 Page 127 of 172
I
I
I
Definitions/Glossary
Client: Energy Laboratories, Inc.
Project/Site: 11 ( e) Byproduct Material
Job ID: 280-127755-2
Qualifiers
Metals
Qualifier
J
Glossary
Abbreviation
I]
%R
CFL
CNF
DER
Dil Fae
DL
DL, RA, RE, IN
DLC
EDL
LOD
LOQ
MDA
MDC
MDL
ML
NC
ND
PQL
QC
RER
RL
RPD
TEF
TEQ
Qualifier Description
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
These commonly used abbreviations may or may not be present in this report.
Listed under the 11D11 column to designate that the result is rep_o_rt-ed~on_a_d_ry_w-ei-g-ht_b_a_s-is-----------------
Percent Recovery
Contains Free Liquid
Contains No Free Liquid
Duplicate Error Ratio (normalized absolute difference)
Dilution Factor
Detection Limit (DoD/DOE)
Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
Decision Level Concentration (Radiochemistry)
Estimated Detection Limit (Dioxin)
Limit of Detection (DoD/DOE)
Limit of Quantitation (DoD/DOE)
Minimum Detectable Activity (Radiochemistry)
Minimum Detectable Concentration (Radiochemistry)
Method Detection Limit
Minimum Level (Dioxin)
Not Calculated
Not Detected at the reporting limit (or MDL or EDL if shown)
Practical Quantitation Limit
Quality Control
Relative Error Ratio (Radiochemistry)
Reporting Limit or Requested Limit (Radiochemistry)
Relative Percent Difference, a measure of the relative difference between two points
Toxicity Equivalent Factor (Dioxin)
Toxicity Equivalent Quotient (Dioxin)
Page 3 of 31
Eurofins TestAmerica, Denver
Page 128 of 172
I
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Job ID: 280-127755-2
Laboratory: Eurofins TestAmerica, Denver
Narrative
Case Narrative
CASE NARRATIVE
Client: Energy Laboratories, Inc.
Project: 11 (e) Byproduct Material
Report Number: 280-127755-2 -Revision 1
Job ID: 280-127755-2
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
This revision adds results for Sn.
RECEIPT
The samples were received on 8/28/2019 10:45 AM ; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperatures of the 3 coolers at receipt time were 2.5° C, 2.8° C and 7.6° C.
Receipt Exceptions
The following sample was received by the laboratory; however, it was not listed on the Chain-of-Custody (COC): M3-54865
(280-127755-25). The sample was logged per the information stated on the sample container.
The following samples were received at the laboratory outside the required temperature criteria: C19081073-005D (280-127755-14),
C19081073-006D (280-127755-17), C19081073-007D (280-127755-20), and C19081073-008D (280-127755-23).
DISSOLVED METALS (ltP/MS)
Samples C19081073-001C (280-127755-1), C19081073-002C (280-127755-4), C19081073-003C (280-127755-7), C19081073-004C
(280-127755-10), C19081073-005C (280-127755-13), C19081073-006C (280-127755-16), C19081073-007C (280-127755-19),
C19081073-008C (280-127755-22) and M3-54865 (280-127755-25) were analyzed for Dissolved Metals (ICP/MS) in accordance with
200.8. The samples were prepared on 10/24/2019 and analyzed on 10/26/2019 and 10/29/2019.
Preparation Batch 160-447588, Analytical Batch 160-447983:
The serial dilution was outside control limits for Calcium indicating a potential matrix interference. : (240-119832-R-1-C SD)
The MS/MSD/serial dilution was analyzed on a different job within the preparation batch. The sample chosen for batch QC had a different
analyte list and QC requirements. As a result, the MS/MSD/serial dilution for Arsenic, Cobalt, Copper, Iron, Manganese, Molybdenum,
Nickel, Selenium, and Zinc was not applied to this job. Method performance is demonstrated by acceptable LCS recovery:
(240-119832-R-1-D MS), (240-119832-R-1-E MSD), and (240-119832-R-1-C SD).
The following samples were diluted to bring the concentration of target analytes within the calibration range. Elevated reporting limits
(Rls) are provided: C19081073-002C (280-127755-4), C19081073-003C (280-127755-7), C19081073-004C (280-127755-10),
C19081073-005C (280-127755-13), C19081073-006C (280-127755-16), C19081073-007C (280-127755-19), and C19081073-008C
(280-127755-22).
Page 4 of 31 Eurofins TestAmerica, Denver
Page 129 of 172
I
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Job ID: _280-127755-2 (Continued) ____ _
Case Narrative
Laboratory: Eurofins TestAmerica, Denver (Continued)
Preparation Batch 160-447588, Analytical Batch 160-448112:
Job ID: 280-127755-2
Due to insufficient sample volume a dilution was performed for the following samples: C19081073-001C (280-127755-1),
C19081073-005C (280-127755-13), C19081073-006C (280-127755-16), C19081073-007C (280-127755-19), and C19081073-008C
(280-127755-22).
The following samples were diluted to bring the concentration of target analytes within the calibration range. In addition, the samples
caused internal standard failure when analyzed at a lesser dilution. Elevated reporting limits (Rls) are provided: C19081073-001C
(280-127755-1), C19081073-002C (280-127755-4), C19081073-003C (280-127755-7), C19081073-004C (280-127755-10),
C19081073-005C (280-127755-13), C19081073-006C (280-127755-16), C19081073-007C (280-127755-19), and C19081073-008C
(280-127755-22).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Page 5 of 31
Eurofins TestAmerica, Denver
Page 130 of 172
I
Detection Summary
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
Project/Site: 11 (e) Byproduct Material
Client Sample ID: C19081073-001C Lab Sample ID: 280-127755-1
Analyte Result Qualifier RL MDL Unit Dil Fae D Method Prep Type
Molybdenum 120 1.8 0.74 mg/L ~ 200.8 Dissolved
Uranium 81 0.37 0.15 mg/L 500 200.8 Dissolved I Arsenic 270 3.7 1.5 mg/L 500 200.8 Dissolved
Beryllium 0.93 0.18 0.074 mg/L 500 200.8 Dissolved
Cadmium 5.4 0.18 0.074 mg/L 500 200.8 Dissolved
Calcium 720 74 35 mg/L 500 200.8 Dissolved
Chromium 15 3.7 1.5 mg/L 500 200.8 Dissolved
Cobalt 66 0.74 0.33 mg/L 500 200.8 Dissolved
Copper 1700 1.1 0.70 mg/L 500 200.8 Dissolved
Iron 9100 18 7.4 mg/L 500 200.8 Dissolved
Lead 22 1.1 0.37 mg/L 500 200.8 Dissolved
Magnesium 9200 18 7.4 mg/L 500 200.8 Dissolved
Manganese 540 1.5 0.55 mg/L 500 200.8 Dissolved
Nickel 110 1.8 0.74 mg/L 500 200.8 Dissolved
Potassium 2600 37 17 mg/L 500 200.8 Dissolved
Sodium 28000 37 18 mg/L 500 200.8 Dissolved
Selenium 10 1.8 0.74 mg/L 500 200.8 Dissolved
Silver 0.79 0.74 0.33 mg/L 500 200.8 Dissolved
Vanadium 1400 3.7 1.5 mg/L 500 200.8 Dissolved
Zinc 550 7.4 2.8 mg/L 500 200.8 Dissolved
Tin 0.54 J 0.74 0.44 mg/L 500 200.8 Dissolved
Client Sample ID: C19081073-002C Lab Sample ID: 280-127755-4
Analyte Result Qualifier RL MDL Unit Dil Fae D Method Prep Type
Molybdenum 0.13 0.050 mg/L --50 -200.8 Dissolved 3.2
Uranium 29 0.025 0.010 mg/L 50 200.8 Dissolved
Arsenic 23 0.25 0.10 mg/L 50 200.8 Dissolved
Beryllium 0.28 0.013 0.0050 mg/L 50 200.8 Dissolved
Cadmium 6.5 0.013 0.0050 mg/L 50 200.8 Dissolved
Calcium 480 5.0 2.4 mg/L 50 200.8 Dissolved
Chromium 2.1 0.25 0.10 mg/L 50 200.8 Dissolved
Cobalt 54 0.050 0.023 mg/L 50 200.8 Dissolved
Copper 160 0.75 0.48 mg/L 500 200.8 Dissolved
Iron 3600 1.3 0.50 mg/L 50 200.8 Dissolved
Lead 0.59 0.075 0.025 mg/L 50 200.8 Dissolved
Magnesium 3700 1.3 0.50 mg/L 50 200.8 Dissolved
Manganese 170 0.10 0.038 mg/L 50 200.8 Dissolved
Nickel 140 1.3 0.50 mg/L 500 200.8 Dissolved
Potassium 710 2.5 1.1 mg/L 50 200.8 Dissolved
Sodium 4600 2.5 1.3 mg/L 50 200.8 Dissolved
Selenium 1.3 0.13 0.050 mg/L 50 200.8 Dissolved
Thallium 0.39 0.050 0.023 mg/L 50 200.8 Dissolved
Vanadium 500 2.5 1.0 mg/L 500 200.8 Dissolved
Zinc 850 5.0 1.9 mg/L 500 200.8 Dissolved
---Client Sample ID: C19081073-003C Lab Sample ID: 280-127755-7
Analyte Result Qualifier RL MDL Unit Dil Fae D Method Prep Type
Molybdenum 0.55 0.13 0.050 mg/L 50 200.8 Dissolved
Uranium 19 0.025 0.010 mg/L 50 200.8 Dissolved
Arsenic 0.38 0.25 0.10 mg/L 50 200.8 Dissolved
This Detection Summary does not include radiochemical test results.
Eurofins TestAmerica, Denver
Page 6 of 31 Page 131 of 172
Detection Summary
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
Project/Site: 11 (e) Byproduct Material
Client Sample ID: C19081073-003C (Continued) Lab Sample ID: 280-127755-7
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Beryllium 0.35 0.13 0.050 mg/L ~ -200.8 Dissolved
Cadmium 7.4 0.013 0.0050 mg/L 50 200.8 Dissolved I Calcium 510 5.0 2.4 mg/L 50 200.8 Dissolved
Chromium 0.23 J 0.25 0.10 mg/L 50 200.8 Dissolved
Cobalt 64 0.050 0.023 mg/L 50 200.8 Dissolved
Copper 35 0,075 0.048 mg/L 50 200.8 Dissolved
Iron 2500 1.3 0.50 mg/L 50 200.8 Dissolved
Magnesium 10000 13 5.0 mg/L 500 200.8 Dissolved
Manganese 1000 1.0 0.38 mg/L 500 200.8 Dissolved
Nickel 150 1.3 0.50 mg/L 500 200.8 Dissolved
Potassium 630 2.5 1.1 mg/L 50 200.8 Dissolved
Sodium 14000 25 13 mg/L 500 200.8 Dissolved
Selenium 2.9 0.13 0.050 mg/L 50 200.8 Dissolved
Silver 0.11 0.050 0.023 mg/L 50 200.8 Dissolved
Thallium 0.17 0.050 0.023 mg/L 50 200.8 Dissolved
Vanadium 54 0.25 0.10 mg/L 50 200.8 Dissolved
Zinc 950 5.0 1.9 mg/L 500 200.8 Dissolved
Client Sample ID: C19081073-004C Lab Sample ID: 280-127755-10
Analyte Result Qualifier RL MDL Unit OIi Fae D Method Prep Type
Molybdenum 19 0.13 0.050 mg/L ~-200.8 Dissolved
Uranium 35 0.025 0.010 mg/L 50 200.8 Dissolved
Arsenic 63 0.25 0.10 mg/L 50 200.8 Dissolved
Beryllium 0.42 0.013 0.0050 mg/L 50 200.8 Dissolved
Cadmium 2.5 0.013 0.0050 mg/L 50 200.8 Dissolved
Calcium 510 50 24 mg/L 500 200.8 Dissolved
Chromium 7.2 2.5 1.0 mg/L 500 200.8 Dissolved
Cobalt 28 0.050 0.023 mg/L 50 200.8 Dissolved
Copper 580 0.75 0.48 mg/L 500 200.8 Dissolved
Iron 3200 1.3 0.50 mg/L 50 200.8 Dissolved
Lead 9.0 0.075 0.025 mg/L 50 200.8 Dissolved
Magnesium 4100 13 5.0 mg/L 500 200.8 Dissolved
Manganese 210 0.10 0.038 mg/L 50 200.8 Dissolved
Nickel 50 0.13 0.050 mg/L 50 200.8 Dissolved
Potassium 1200 25 11 mg/L 500 200.8 Dissolved
Sodium 15000 25 13 mg/L 500 200.8 Dissolved
Selenium 3.7 0.13 0.050 mg/L 50 200.8 Dissolved
Silver 0.31 0.050 0.023 mg/L 50 200.8 Dissolved
Thallium 0.090 0.050 0.023 mg/L 50 200.8 Dissolved
Vanadium 150 2.5 1.0 mg/L 500 200.8 Dissolved
Zinc 280 5.0 1.9 mg/L 500 200.8 Dissolved
Tin 0.077 0.050 0.030 mg/L 50 200.8 Dissolved
Client Sample ID: C19081073-005C Lab Sample ID: 280-127755-J 3
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Molybdenum 8.4 0.18 0.071 mg/L --5-0 200.8 Dissolved
Uranium 38 0.036 0.014 mg/L 50 200.8 Dissolved
Arsenic 52 0.36 0.14 mg/L 50 200.8 Dissolved
Beryllium 0.37 0.018 0.0071 mg/L 50 200.8 Dissolved
Cadmium 1.9 0.018 0.0071 mg/L 50 200.8 Dissolved
This Detection Summary does not include radiochemical test results.
Eurofins TestAmerica, Denver
Page 7 of 31 Page 132 of 172
Detection Summary
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
Project/Site: 11 (e) Byproduct Material
Client Sample ID: C19081073-005C (Continued) Lab Sample ID: 280-127755-13
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Calcium 520 71 34 mg/L 500 200.8 Dissolved
Chromium 6.5 3.6 1.4 mg/L 500 200.8 Dissolved I Cobalt 25 0.071 0.032 mg/L 50 200.8 Dissolved
Copper 500 1.1 0.68 mg/L 500 200.8 Dissolved
Iron 2500 1.8 0.71 mg/L 50 200.8 Dissolved
Lead 4.2 0.11 0.036 mg/L 50 200.8 Dissolved
Magnesium 3800 18 7.1 mg/L 500 200.8 Dissolved
Manganese 190 0.14 0.054 mg/L 50 200.8 Dissolved
Nickel 46 0.18 0.071 mg/L 50 200.8 Dissolved
Potassium 1000 36 16 mg/L 500 200.8 Dissolved
Sodium 13000 36 18 mg/L 500 200.8 Dissolved
Selenium 3.1 0.18 0.071 mg/L 50 200.8 Dissolved
Silver 0.23 0.071 0.032 mg/L 50 200.8 Dissolved
Thallium 0.055 J 0.071 0.032 mg/L 50 200.8 Dissolved
Vanadium 130 3.6 1.4 mg/L 500 200.8 Dissolved
Zinc 210 0.71 0.27 mg/L 50 200.8 Dissolved
Client Sample ID: C19081073-006C Lab Sample ID: 280-127755-16
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Molybdenum 29 0.25 0.10 mg/L 50 -200.8 Dissolved
Uranium 36 0.050 0.020 mg/L 50 200.8 Dissolved
Arsenic 140 0.50 0.20 mg/L 50 200.8 Dissolved
Beryllium 0.64 0.025 0.010 mg/L 50 200.8 Dissolved
Cadmium 2.0 0.025 0.010 mg/L 50 200.8 Dissolved
Calcium 670 100 48 mg/L 500 200.8 Dissolved
Chromium 12 5.0 2.0 mg/L 500 200.8 Dissolved
Cobalt 44 0.10 0.045 mg/L 50 200.8 Dissolved
Copper 830 1.5 0.95 mg/L 500 200.8 Dissolved
Iron 5800 2.5 1.0 mg/L 50 200.8 Dissolved
Lead 16 0.15 0.050 mg/L 50 200.8 Dissolved
Magnesium 6500 25 10 mg/L 500 200.8 Dissolved
Manganese 320 0.20 O.Q75 mg/L 50 200.8 Dissolved
Nickel 78 0.25 0.10 mg/L 50 200.8 Dissolved
Potassium 1900 50 23 mg/L 500 200.8 Dissolved
Sodium 18000 50 25 mg/L 500 200.8 Dissolved
Selenium 6.6 0.25 0.10 mg/L 50 200.8 Dissolved
Silver 0.17 0.10 0.045 mg/L 50 200.8 Dissolved
Vanadium 710 5.0 2.0 mg/L 500 200.8 Dissolved
Zinc 280 1.0 0.38 mg/L 50 200.8 Dissolved
Tin 0.34 0.10 0.060 mg/L 50 200.8 Dissolved
Client Sample ID: C19081073-007C Lab Sample ID: 280-127755-19
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Molybdenum 27 0.25 0.10 mg/L --5-0 200.8 Dissolved
Uranium 31 0.050 0.020 mg/L 50 200.8 Dissolved
Arsenic 89 0.50 0.20 mg/L 50 200.8 Dissolved
Beryllium 0.47 0.025 0.010 mg/L 50 200.8 Dissolved
Cadmium 2.0 0.025 0.010 mg/L 50 200.8 Dissolved
Calcium 550 100 48 mg/L 500 200.8 Dissolved
Chromium 9.1 5.0 2.0 mg/L 500 200.8 Dissolved
This Detection Summary does not include radiochemical test results.
Eurofins TestAmerica, Denver
Page 8 of 31 Page 133 of 172
Detection Summary
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
Project/Site: 11(e) Byproduct Material
Client Sample ID: C19081073-007C (Continued) Lab Sample ID: 280-127755-19
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Cobalt 31 0.10 0.045 mg/L ~ -200.8 Dissolved
Copper 550 1.5 0.95 mg/L 500 200.8 Dissolved I Iron 4400 2.5 1.0 mg/L 50 200.8 Dissolved
Lead 7.8 0.15 0.050 mg/L 50 200.8 Dissolved
Magnesium 4800 25 10 mg/L 500 200.8 Dissolved
Manganese 240 0.20 0.075 mg/L 50 200.8 Dissolved
Nickel 59 0.25 0.10 mg/L 50 200.8 Dissolved
Potassium 1400 50 23 mg/L 500 200.8 Dissolved
Sodium 13000 50 25 mg/L 500 200.8 Dissolved
Selenium 4.7 0.25 0.10 mg/L 50 200.8 Dissolved
Silver 0.17 0.10 0.045 mg/L 50 200.8 Dissolved
Thallium 0.087 J 0.10 0.045 mg/L 50 200.8 Dissolved
Vanadium 760 5.0 2.0 mg/L 500 200.8 Dissolved
Zinc 280 1.0 0.38 mg/L 50 200.8 Dissolved
Tin 0.20 0.10 0.060 mg/L 50 200.8 Dissolved
Client Sample ID: C19081073-008C Lab Sample ID: 280-127755-22
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Molybdenum 110 0.63 0.25 mg/L --5-0 200.8 Dissolved
Uranium 77 0.13 0.050 mg/L 50 200.8 Dissolved
Arsenic 230 1.3 0.50 mg/L 50 200.8 Dissolved
Beryllium 0.90 0.063 0.025 mg/L 50 200.8 Dissolved
Cadmium 4.8 0.063 0.025 mg/L 50 200.8 Dissolved
Calcium 620 25 12 mg/L 50 200.8 Dissolved
Chromium 12 1.3 0.50 mg/L 50 200.8 Dissolved
Cobalt 60 0.25 0.11 mg/L 50 200.8 Dissolved
Copper 1500 3.8 2.4 mg/L 500 200.8 Dissolved
Iron 7800 6.3 2.5 mg/L 50 200.8 Dissolved
Lead 22 0.38 0.13 mg/L 50 200.8 Dissolved
Magnesium 7000 6.3 2.5 mg/L 50 200.8 Dissolved
Manganese 470 0.50 0.19 mg/L 50 200.8 Dissolved
Nickel 90 0.63 0.25 mg/L 50 200.8 Dissolved
Potassium 1900 13 5.6 mg/L 50 200.8 Dissolved
Sodium 21000 13 6.3 mg/L 50 200.8 Dissolved
Selenium 7.9 0.63 0.25 mg/L 50 200.8 Dissolved
Silver 0.69 0.25 0.11 mg/L 50 200.8 Dissolved
Thallium 0.13 J 0.25 0.11 mg/L 50 200.8 Dissolved
Vanadium 1300 13 5.0 mg/L 500 200.8 Dissolved
Zinc 490 2.5 0.94 mg/L 50 200.8 Dissolved
Tin 0.46 0.25 0.15 mg/L 50 200.8 Dissolved
Client Sample ID: M3-54865 Lab Sample ID: 280-127755-25
Analyte Result Qualifier RL MDL Unit Oil Fae D Method Prep Type
Uranium 0.0015 0.0010 0.00040 mg/L --2 200.8 Dissolved
Calcium 0.22 0.20 0.096 mg/L 2 200.8 Dissolved
Cobalt 0.0011 J 0.0020 0.00090 mg/L 2 200.8 Dissolved
Copper 0.021 0.0030 0.0019 mg/L 2 200.8 Dissolved
Iron 0.12 0.050 0.020 mg/L 2 200.8 Dissolved
Magnesium 0.18 0.050 0.020 mg/L 2 200.8 Dissolved
Manganese 0.0084 0.0040 0.0015 mg/L 2 200.8 Dissolved
This Detection Summary does not include radiochemical test results.
Eurofins TestAmerica, Denver
Page 9 of 31 Page 134 of 172
Detection Summary
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Client Sample ID: M3-54865 (Continued)
Analyte Result Qualifier RL MDL
Nickel 0.0022 J 0.0050 0.0020
Potassium 0.048 J 0.10 0.045
Sodium 0.62 0.10 0.050
Vanadium 0.0063 J 0.010 0.0040
Zinc 0.014 J 0.020 0.0075
This Detection Summary does not include radiochemical test results.
Page 10 of 31
Job ID: 280-127755-2
Lab Sample ID: 280-127755-25
Unit OIi Fae D Method Prep Type
mg/L --2 -200.8 Dissolved
mg/L 2 200.8 Dissolved I mg/L 2 200.8 Dissolved
mg/L 2 200.8 Dissolved
mg/L 2 200.8 Dissolved
Eurofins TestAmerica, Denver
Page 135 of 172
Client: Energy Laboratories, Inc.
ProjecUSite: 11 (e) Byproduct Material
Method 200.8 __ _
200.7/200.8
Method Description
ICPMS Dissolved Metals by 200.8
Preparation, Metals
Protocol References:
EPA= US Environmental Protection Agency
Laboratory References:
Method Summary
TAL SL= Eurofins TestAmerica, St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Page 11 of 31
Job ID: 280-127755-2
Protocol
EPA ----
EPA
Laboratory
TAL SL
TALSL
Eurofins TestAmerica, Denver
Page 136 of 172
I
Client: Energy Laboratories, Inc.
Project/Site: 11(e) Byproduct Material
Lab Sample ID Client Sample ID
280-127755-1 C19081073-001C
280-1 27755-4 C 19081073-002C
280-127755-7 C 19081073-003C
280-127755-10 C 19081073-004C
280-127755-13 C 19081073-005C
280-127755-16 C 19081073-006C
280-127755-19 C 19081 073-007C
280-127755-22 C19081073-008C
280-127755-25 M3-54865
Sample Summary
Job ID: 280-127755-2
Matrix Collected Received Asset ID
Water 08/21/19 08:35 08/28/19 10:45
Water 08/21/19 09:05 08/28/19 10:45
Water 08/21/19 09:20 08/28/19 10:45
Water 08/21/19 09:40 08/28/19 10:45
Water 08/21/19 09:45 08/28/19 10:45
Water 08/21/19 10:15 08/28/19 10:45
Water 08/21/19 10:30 08/28/19 10:45 I Water 08/21/19 08:35 08/28/19 10:45
Water 08/23/19 11 :20 08/28/19 10:45
Eurofins TestAmerica, Denver
Page 12 of 31 Page 137 of 172
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
ProjecUSite: 11 (e) Byproduct Material
Method: 200.8 -ICPMS Dissolved Metals by 200.8 -Dissolved
Client Sample ID: C19081073-001C Lab Sample ID: 280-127755-1
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Molybdenum 120 1.8 ~ mg/L 10/24/19 13:54 10/29/19 01 :25 ~
Uranium 81 0.37 0.15 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Arsenic 270 3.7 1.5 mg/L 10/24/19 13:54 10/29/19 01:25 500
Beryllium 0.93 0.18 0.074 mg/L 10/24/19 13:54 10/29/19 01:25 500
Cadmium 5.4 0.18 0.074 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Calcium 720 74 35 mg/L 10/24/19 13:54 10/29/19 01 :25 500 I Chromium 15 3.7 1.5 mg/L 10/24/19 13:54 10/29/19 01:25 500
Cobalt 66 0.74 0.33 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Copper 1700 1.1 0.70 mg/L 10/24/19 13:54 10/29/19 01:25 500
Iron 9100 18 7.4 mg/L 10/24/19 13:54 10/29/1901 :25 500
Lead 22 1.1 0.37 mg/L 10/24/19 13:54 10/29/19 01:25 500
Magnesium 9200 18 7.4 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Manganese 540 1.5 0.55 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Nickel 110 1.8 0.74 mg/L 10/24/19 13:54 10/29/19 01:25 500
Potassium 2600 37 17 mg/L 10/24/19 13:54 10/29/19 01:25 500
Sodium 28000 37 18 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Selenium 10 1.8 0.74 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Silver 0.79 0.74 0.33 mg/L 10/24/19 13:54 10/29/19 01:25 500
Thallium ND 0.74 0.33 mg/L 10/24/19 13:54 10/29/19 01:25 500
Vanadium 1400 3.7 1.5 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Zinc 550 7.4 2.8 mg/L 10/24/19 13:54 10/29/19 01 :25 500
Tin 0.54 J 0.74 0.44 mg/L 10/24/19 13:54 10/29/19 01:25 500
Client Sample ID: C19081073-002C Lab Sample ID: 280-127755-4
Date Collected: 08/21/19 09:05 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Molybdenum 3.2 0.13 0.050 mg/L 10/24/19 13:54 10/26/19 06:24 ~
Uranium 29 0.025 0.010 mg/L 10/24/19 13:54 10/26/19 06:24 50
Arsenic 23 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:24 50
Beryllium 0.28 0.013 0.0050 mg/L 10/24/19 13:54 10/26/19 06:24 50
Cadmium 6.5 0.013 0.0050 mg/L 10/24/19 13:54 10/26/19 06:24 50
Calcium 480 5.0 2.4 mg/L 10/24/19 13:54 10/26/19 06:24 50
Chromium 2.1 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:24 50
Cobalt 54 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:24 50
Copper 160 0.75 0.48 mg/L 10/24/19 13:54 10/29/1901 :31 500
Iron 3600 1.3 0.50 mg/L 10/24/19 13:54 10/26/19 06:24 50
Lead 0.59 0.075 0.025 mg/L 10/24/19 13:54 10/26/19 06:24 50
Magnesium 3700 1.3 0.50 mg/L 10/24/19 13:54 10/26/19 06:24 50
Manganese 170 0.10 0.038 mg/L 10/24/19 13:54 10/26/19 06:24 50
Nickel 140 1.3 0.50 mg/L 10/24/19 13:54 10/29/19 01:31 500
Potassium 710 2.5 1.1 mg/L 10/24/19 13:54 10/26/19 06:24 50
Sodium 4600 2.5 1.3 mg/L 10/24/19 13:54 10/26/19 06:24 50
Selenium 1.3 0.13 0.050 mg/L 10/24/19 13:54 10/26/19 06:24 50
Silver ND 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:24 50
Thallium 0.39 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:24 50
Vanadium 500 2.5 1.0 mg/L 10/24/19 13:54 10/29/1901 :31 500
Zinc 850 5.0 1.9 mg/L 10/24/19 13:54 10/29/19 01:31 500
Tin ND 0.050 0.030 mg/L 10/24/19 13:54 10/26/19 06:24 50
Eurofins TestAmerica, Denver
Page 13 of 31 Page 138 of 172
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
ProjecUSite: 11 (e) Byproduct Material
Method: 200.8 -ICPMS Dissolved Metals by 200.8 -Dissolved
Client Sample ID: C19081073-003C Lab Sample ID: 280-127755-7
Date Collected: 08/21/19 09:20 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Molybdenum 0.55 0:13 0.050 mg/L 10/24/19 13:54 10/26/19 06:31 50
Uranium 19 0.025 0.010 mg/L 10/24/19 13:54 10/26/19 06:31 50
Arsenic 0.38 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:31 50
Beryllium 0.35 0.13 0.050 mg/L 10/24/19 13:54 10/29/19 01 :38 500
Cadmium 7.4 0.013 0.0050 mg/L 10/24/19 13:54 10/26/19 06:31 50
Calcium 510 5.0 2.4 mg/L 10/24/19 13:54 10/26/19 06:31 50 I Chromium 0.23 J 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:31 50
Cobalt 64 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:31 50
Copper 35 0.075 0.048 mg/L 10/24/19 13:54 10/26/19 06:31 50
Iron 2500 1.3 0.50 mg/L 10/24/19 13:54 10/26/19 06:31 50
Lead ND 0.075 0.025 mg/L 10/24/19 13:54 10/26/19 06:31 50
Magnesium 10000 13 5.0 mg/L 10/24/19 13:54 10/29/1901 :38 500
Manganese 1000 1.0 0.38 mg/L 10/24/19 13:54 10/29/1901 :38 500
Nickel 150 1.3 0.50 mg/L 10/24/19 13:54 10/29/19 01 :38 500
Potassium 630 2.5 1.1 mg/L 10/24/19 13:54 10/26/19 06:31 50
Sodium 14000 25 13 mg/L 10/24/19 13:54 10/29/1901 :38 500
Selenium 2.9 0.13 0.050 mg/L 10/24/19 13:54 10/26/19 06:31 50
Silver 0.11 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:31 50
Thallium 0.17 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:31 50
Vanadium 54 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:31 50
Zinc 950 5.0 1.9 mg/L 10/24/19 13:54 10/29/1901 :38 500
Tin ND 0.050 0.030 mg/L 10/24/19 13:54 10/26/19 06:31 50
Client Sample ID: C19081073-004C Lab Sample ID: 280-127755-10
Date Collected: 08/21/19 09:40 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Molybdenum 19 0.13 0.050 mg/L 10/24/19 13:54 10/26/19 06:37 --5-0
Uranium 35 0.025 0.010 mg/L 10/24/19 13:54 10/26/19 06:37 50
Arsenic 63 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:37 50
Beryllium 0.42 0.013 0.0050 mg/L 10/24/19 13:54 10/26/19 06:37 50
Cadmium 2.5 0.013 0.0050 mg/L 10/24/19 13:54 10/26/19 06:37 50
Calcium 510 50 24 mg/L 10/24/19 13:54 10/29/19 01 :45 500
Chromium 7.2 2.5 1.0 mg/L 10/24/19 13:54 10/29/19 01:45 500
Cobalt 28 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:37 50
Copper 580 0.75 0.48 mg/L 10/24/19 13:54 10/29/1901 :45 500
Iron 3200 1.3 0.50 mg/L 10/24/19 13:54 10126/19 06:37 50
Lead 9.0 0.075 0.025 mg/L 10/24/19 13:54 10/26/19 06:37 50
Magnesium 4100 13 5.0 mg/L 10/24/19 13:54 10/29/19 01 :45 500
Manganese 210 0.10 0.038 mg/L 10/24/19 13:54 10/26/19 06:37 50
Nickel 50 0.13 0.050 mg/L 10/24/19 13:54 10/26/19 06:37 50
Potassium 1200 25 11 mg/L 10/24/19 13:54 10/29/1901 :45 500
Sodium 15000 25 13 mg/L 10/24/19 13:54 10/29/1901 :45 500
Selenium 3.7 0.13 0.050 mg/L 10/24/19 13:54 10/26/19 06:37 50
Silver 0.31 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:37 50
Thallium 0.090 0.050 0.023 mg/L 10/24/19 13:54 10/26/19 06:37 50
Vanadium 150 2.5 1.0 mg/L 10/24/19 13:54 10/29/19 01 :45 500
Zinc 280 5.0 1.9 mg/L 10/24/19 13:54 10/29/1901 :45 500
Tin 0.077 0.050 0.030 mg/L 10/24/19 13:54 10/26/19 06:37 50
Eurofins TestAmerica, Denver
Page 14 of 31 Page 139 of 172
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
Project/Site: 11 (e) Byproduct Material
Method: 200.8 -ICPMS Dissolved Metals by 200.8 -Dissolved
Client Sample ID: C19081073-005C Lab Sample ID: 280-127755-13
Date Collected: 08/21/19 09:45 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Molybdenum 8.4 0.18 0.071 mg/L 10/24/19 13:54 10/26/19 06:44 --5-0
Uranium 38 0.036 0.014 mg/L 10/24/19 13:54 10/26/19 06:44 50
Arsenic 52 0.36 0.14 mg/L 10/24/19 13:54 10/26/19 06:44 50
Beryllium 0.37 0.018 0.0071 mg/L 10/24/19 13:54 10/26/19 06:44 50
Cadmium 1.9 0.018 0.0071 mg/L 10/24/19 13:54 10/26/19 06:44 50
Calcium 520 71 34 mg/L 10/24/19 13:54 10/29/19 01 :51 500 I Chromium 6.5 3.6 1.4 mg/L 10/24/19 13:54 10/29/19 01 :51 500
Cobalt 25 0.071 0.032 mg/L 10/24/1913:54 10/26/19 06:44 50
Copper 500 1.1 0.68 mg/L 10/24/19 13:54 10/29/1901 :51 500
Iron 2500 1.8 0.71 mg/L 10/24/19 13:54 10/26/19 06:44 50
Lead 4.2 0.11 0.036 mg/L 10/24/19 13:54 10/26/19 06:44 50
Magnesium 3800 18 7.1 mg/L 10/24/19 13:54 10/29/19 01 :51 500
Manganese 190 0.14 0.054 mg/L 10/24/19 13:54 10/26/19 06:44 50
Nickel 46 0.18 0.071 mg/L 10/24/19 13:54 10/26/19 06:44 50
Potassium 1000 36 16 mg/L 10/24/19 13:54 10/29/19 01 :51 500
Sodium 13000 36 18 mg/L 10/24/19 13:54 10/29/19 01 :51 500
Selenium 3.1 0.18 0.071 mg/L 10/24/19 13:54 10/26/19 06:44 50
Silver 0.23 0.071 0.032 mg/L 10/24/19 13:54 10/26/19 06:44 50
Thallium 0.055 J 0.071 0.032 mg/L 10/24/19 13:54 10/26/19 06:44 50
Vanadium 130 3.6 1.4 mg/L 10/24/19 13:54 10/29/19 01 :51 500
Zinc 210 0.71 0.27 mg/L 10/24/19 13:54 10/26/19 06:44 50
Tin ND 0.071 0.043 mg/L 10/24/19 13:54 10/26/19 06:44 50
Client Sample ID: C19081073-006C Lab Sample ID: 280-127755-16
Date Collected: 08/21/19 10:15 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Molybdenum 29 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:51 50
Uranium 36 0.050 0.020 mg/L 10/24/19 13:54 10/26/19 06:51 50
Arsenic 140 0.50 0.20 mg/L 10/24/19 13:54 10/26/19 06:51 50
Beryllium 0.64 0.025 0.010 mg/L 10/24/19 13:54 10/26/19 06:51 50
Cadmium 2.0 0.025 0.010 mg/L 10/24/19 13:54 10/26/19 06:51 50
Calcium 670 100 48 mg/L 10/24/19 13:54 10/29/19 01 :58 500
Chromium 12 5.0 2.0 mg/L 10/24/19 13:54 10/29/19 01 :58 500
Cobalt 44 0.10 0.045 mg/L 10/24/19 13:54 10/26/19 06:51 50
Copper 830 1.5 0.95 mg/L 10/24/19 13:54 10/29/1901 :58 500
Iron 5800 2.5 1.0 mg/L 10/24/19 13:54 10/26/19 06:51 50
Lead 16 0.15 0.050 mg/L 10/24/19 13:54 10/26/19 06:51 50
Magnesium 6500 25 10 mg/L 10/24/19 13:54 10/29/19 01 :58 500
Manganese 320 0.20 0.075 mg/L 10/24/19 13:54 10/26/19 06:51 50
Nickel 78 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:51 50
Potassium 1900 50 23 mg/L 10/24/19 13:54 10/29/19 01 :58 500
Sodium 18000 50 25 mg/L 10/24/19 13:54 10/29/19 01 :58 500
Selenium 6.6 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:51 50
Silver 0.17 0.10 0.045 mg/L 10/24/19 13:54 10/26/19 06:51 50
Thallium ND 0.10 0.045 mg/L 10/24/19 13:54 10/26/19 06:51 50
Vanadium 710 5.0 2.0 mg/L 10/24/19 13:54 10/29/19 01 :58 500
Zinc 280 1.0 0.38 mg/L 10/24/19 13:54 10/26/19 06:51 50
Tin 0.34 0.10 0.060 mg/L 10/24/19 13:54 10/26/19 06:51 50
Eurofins TestAmerica, Denver
Page 15 of 31 Page 140 of 172
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
Project/Site: 11(e) Byproduct Material
Method: 200.8 -ICPMS Dissolved Metals by 200.8 -Dissolved
Client Sample ID: C19081073-007C Lab Sample ID: 280-127755-19
Date Collected: 08/21/19 10:30 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Molybdenum 27 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:58 --5-0
Uranium 31 0.050 0.020 mg/L 10/24/19 13:54 10/26/19 06:58 50
Arsenic 89 0.50 0.20 mg/L 10/24/19 13:54 10/26/19 06:58 50
Beryllium 0.47 0.025 0.010 mg/L 10/24/19 13:54 10/26/19 06:58 50
Cadmium 2.0 0.025 0.010 mg/L 10/24/19 13:54 10/26/19 06:58 50
Calcium 550 100 48 mg/L 10/24/19 13:54 10/29/19 02:05 500 I Chromium 9.1 5.0 2.0 mg/L 10/24/19 13:54 10/29/19 02:05 500
Cobalt 31 0.10 0.045 mg/L 10/24/19 13:54 10/26/19 06:58 50
Copper 550 1.5 0.95 mg/L 10/24/19 13:54 10/29/19 02:05 500
Iron 4400 2.5 1.0 mg/L 10/24/19 13:54 10/26/19 06:58 50
Lead 7.8 0.15 0.050 mg/L 10/24/19 13:54 10/26/19 06:58 50
Magnesium 4800 25 10 mg/L 10/24/19 13:54 10/29/19 02:05 500
Manganese 240 0.20 0.075 mg/L 10/24/19 13:54 10/26/19 06:58 50
Nickel 59 0.25 0.10 mg/L 10/24/19 13:54 10/26/19 06:58 50
Potassium 1400 50 23 mg/L 10/24/19 13:54 10/29/19 02:05 500
Sodium 13000 50 25 mg/L 10/24/19 13:54 10/29/19 02:05 500
Selenium 4.7 0.25 0.10 mg/L 10/24/1913:54 10/26/19 06:58 50
Silver 0.17 0.10 0.045 mg/L 10/24/19 13:54 10/26/19 06:58 50
Thallium 0.087 J 0.10 0.045 mg/L 10/24/19 13:54 10/26/19 06:58 50
Vanadium 760 5.0 2.0 mg/L 10/24/19 13:54 10/29/19 02:05 500
Zinc 280 1.0 0.38 mg/L 10/24/19 13:54 10/26/19 06:58 50
Tin 0.20 0.10 0.060 mg/L 10/24/19 13:54 10/26/19 06:58 50
Client Sample ID: C19081073-008C Lab Sample ID: 280-127755-22
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Molybdenum 110 0.63 0.25 mg/L 10/24/19 13:54 10/26/19 07:25 ---"so
Uranium 77 0.13 0.050 mg/L 10/24/19 13:54 10/26/19 07:25 50
Arsenic 230 1.3 0.50 mg/L 10/24/19 13:54 10/26/19 07:25 50
Beryllium 0.90 0.063 0.025 mg/L 10/24/19 13:54 10/26/19 07:25 50
Cadmium 4.8 0.063 0.025 mg/L 10/24/19 13:54 10/26/19 07:25 50
Calcium 620 25 12 mg/L 10/24/19 13:54 10/26/19 07:25 50
Chromium 12 1.3 0.50 mg/L 10/24/19 13:54 10/26/19 07:25 50
Cobalt 60 0.25 0.11 mg/L 10/24/19 13:54 10/26/19 07:25 50
Copper 1500 3.8 2.4 mg/L 10/24/19 13:54 10/29/19 02 :12 500
Iron 7800 6.3 2.5 mg/L 10/24/19 13:54 10/26/19 07:25 50
Lead 22 0.38 0.13 mg/L 10/24/19 13:54 10/26/19 07:25 50
Magnesium 7000 6.3 2.5 mg/L 10/24/1913:54 10/26/19 07:25 50
Manganese 470 0.50 0.19 mg/L 10/24/19 13:54 10/26/19 07:25 50
Nickel 90 0.63 0.25 mg/L 10/24/19 13:54 10/26/19 07:25 50
Potassium 1900 13 5.6 mg/L 10/24/19 13:54 10/26/19 07:25 50
Sodium 21000 13 6.3 mg/L 10/24/19 13:54 10/26/19 07:25 50
Selenium 7.9 0.63 0.25 mg/L 10/24/19 13:54 10/26/19 07:25 50
Silver 0.69 0.25 0.11 mg/L 10/24/19 13:54 10/26/19 07:25 50
Thallium 0.13 J 0.25 0.11 mg/L 10/24/19 13:54 10/26/19 07:25 50
Vanadium 1300 13 5.0 mg/L 10/24/19 13:54 10/29/19 02:12 500
Zinc 490 2.5 0.94 mg/L 10/24/19 13:54 10/26/19 07:25 50
Tin 0.46 0.25 0.15 mg/L 10/24/19 13:54 10/26/19 07:25 50
Eurofins TestAmerica, Denver
Page 16 of 31 Page 141 of 172
Client Sample Results
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
ProjecVSite: 11 (e) Byproduct Material
Method: 200.8 -ICPMS Dissolved Metals by 200.8 -Dissolved
Client Sample ID: M3-54865 Lab Sample ID: 280-127755-25
Date Collected: 08/23/19 11 :20 Matrix: Water
Date Received: 08/28/19 10:45
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fae
Molybdenum ND 0.0050 0.0020 mg/L 10/24/19 13:54 10/29/19 02: 18 2
Uranium 0.0015 0.0010 0.00040 mg/L 10/24/19 13:54 10/29/19 02: 18 2
Arsenic ND 0.010 0.0040 mg/L 10/24/19 13:54 10/29/19 02: 18 2
Beryllium ND 0.00050 0.00020 mg/L 10/24/19 13:54 10/29/19 02: 18 2
Cadmium ND 0.00050 0.00020 mg/L 10/24/19 13:54 10/29/19 02:18 2
Calcium 0.22 0.20 0.096 mg/L 10/24/19 13:54 10/29/19 02:18 2 I Chromium ND 0.010 0.0040 mg/L 10/24/19 13:54 10/29/19 02: 18 2
Cobalt 0.0011 J 0.0020 0.00090 mg/L 10/24/19 13:54 10/29/19 02:18 2
Copper 0.021 0.0030 0.0019 mg/L 10/24/19 13:54 10/29/19 02:18 2
Iron 0.12 0.050 0.020 mg/L 10/24/19 13:54 10/29/19 02: 18 2
Lead ND 0.0030 0.0010 mg/L 10/24/19 13:54 10/29/19 02: 18 2
Magnesium 0.18 0.050 0.020 mg/L 10/24/19 13:54 10/29/19 02: 18 2
Manganese 0.0084 0.0040 0.0015 mg/L 10/24/19 13:54 10/29/19 02:18 2
Nickel 0.0022 J 0.0050 0.0020 mg/L 10/24/19 13:54 10/29/19 02:18 2
Potassium 0.048 J 0.10 0.045 mg/L 10/24/19 13:54 10/29/19 02:18 2
Sodium 0.62 0.10 0.050 mg/L 10/24/19 13:54 10/29/19 02:18 2
Selenium ND 0.0050 0.0020 mg/L 10/24/19 13:54 10/29/19 02:18 2
Silver ND 0.0020 0.00090 mg/L 10/24/19 13:54 10/29/19 02:18 2
Thallium ND 0.0020 0.00090 mg/L 10/24/19 13:54 10/29/19 02:18 2
Vanadium 0.0063 J 0.010 0.0040 mg/L 10/24/19 13:54 10/29/19 02: 18 2
Zinc 0.014 J 0.020 0.0075 mg/L 10/24/19 13:54 10/29/19 02: 18 2
Tin ND 0.0020 0.0012 mg/L 10/24/19 13:54 10/29/19 02:18 2
Eurofins TestAmerica, Denver
Page 17 of 31 Page 142 of 172
QC Sample Results
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Method: 200.8 -ICPMS Dissolved Metals by 200.8
Lab Sample ID: MB 160-447588/1-A
Matrix: Water
Analysis Batch: 447983
MB
Analyte Result
Molybdenum
Uranium
Arsenic
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Nickel
Potassium
Sodium
Selenium
Silver
Thallium
Vanadium
Zinc
Tin
Lab Sample ID: LCS 160-447588/2-A
Matrix: Water
Analysis Batch: 447983
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
MB
Qualifier RL
0.0050
0.0010
0.010
0.00050
0.00050
0.20
0.010
0.0020
0.0030
0.050
0.0030
0.050
0.0040
0.0050
0.10
0.10
0.0050
0.0020
0.0020
0.010
0.020
0.0020
Spike
MDL
0.0020
0.00040
0.0040
0.00020
0.00020
0.096
0.0040
0.00090
0.0019
0.020
0.0010
0.020
0.0015
0.0020
0.045
0.050
0.0020
0.00090
0.00090
0.0040
0.0075
0.0012
LCS LCS
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Analyte
Molybdenum
Uranium
Arsenic
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Added Result Qualifier
Iron
Lead
Magnesium
Manganese
Nickel
Potassium
Sodium
Selenium
Silver
Thallium
Vanadium
Zinc
0.500 0.531
1.00 1.05
1.00 0.970
0.100 0.0965
1.00 1.05
10.0 10.5
1.00 0.959
1.00 1.00
1.00 1.01
10.0 9.81
1.00 1.04
10.0 9.86
1.00 1.04
1.00 0.974
10.0 9.60
10.0 9.88
0.500 0.468
0.200 0.205
0.200 0.210
1.00 0.969
1.00 0.948
Page 18 of 31
Job ID: 280-127755-2
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 447588
D Prepared Analyzed Dil Fae
10/24/19 13:54 10/26/19 06:03 --2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2 I 10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
10/24/19 13:54 10/26/19 06:03 2
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 447588
%Rec.
Unit D %Rec Limits -------mg/L 106 85-115
mg/L 105 85-115
mg/L 97 85-115
mg/L 96 85-115
mg/L 105 85-115
mg/L 105 85-115
mg/L 96 85-115
mg/L 100 85-115
mg/L 101 85-115
mg/L 98 85-115
mg/L 104 85-115
mg/L 99 85-115
mg/L 104 85-115
mg/L 97 85-115
mg/L 96 85-115
mg/L 99 85-115
mg/L 94 85-115
mg/L 102 85-115
mg/L 105 85 -115
mg/L 97 85-115
mg/L 95 85-115
Eurofins TestAmerica, Denver
Page 143 of 172
QC Sample Results
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Method: 200.8 -ICPMS Dissolved Metals by 200.8 (Continued)
Lab Sample ID: LCS 160-447588/2-A
Matrix: Water
Analysis Batch: 447983
Spike LCS LCS
Job ID: 280-127755-2
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 447588
%Rec.
Analyte
Tl_n _
Added Result Qualifier Unit D %Rec Limits
-1-:o5 -1.00 mg/L 100 85-115
Eurofins TestAmerica, Denver
Page 19 of 31 Page 144 of 172
I
QC Association Summary
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
Project/Site: 11 (e) Byproduct Material
Metals
Prep Batch: 447588
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
280-127755-1 C19081073-001C Dissolved Water 200.7/200.8
280-127755-4 C 19081 073-002C Dissolved Water 200. 7/200.8
280-127755-7 C 19081073-003C Dissolved Water 200.7/200.8
280-127755-10 C 19081 073-004C Dissolved Water 200.7/200.8
280-127755-13 C19081073-005C Dissolved Water 200.7/200.8
280-127755-16 C 19081073-006C Dissolved Water 200.7/200.8
280-127755-19 C 19081073-007C Dissolved Water 200.7/200.8
280-127755-22 C 19081073-008C Dissolved Water 200.7/200.8
280-127755-25 M3-54865 Dissolved Water 200.7/200.8
MB 160-447588/1-A Method Blank Total/NA Water 200.7/200.8
LCS 160-44 7588/2-A Lab Control Sample Total/NA Water 200.7/200.8
Analysis Batch: 447983 ~
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
280-127755-4 C 19081073-002C Dissolved Water 200.8 447588
280-127755-7 C 19081073-003C Dissolved Water 200.8 447588
280-127755-10 C 19081073-004C Dissolved Water 200.8 447588
280-127755-13 C 19081073-005C Dissolved Water 200.8 447588
280-127755-16 C 19081 073-006C Dissolved Water 200.8 447588
280-127755-19 C19081073-007C Dissolved Water 200.8 447588
280-127755-22 C 19081 073-008C Dissolved Water 200.8 447588
MB 160-447588/1-A Method Blank Total/NA Water 200.8 447588
LCS 160-447588/2-A Lab Control Sample Total/NA Water 200.8 447588
Analysis Batch: 448112
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
280-127755-1 C19081073-001C Dissolved Water 200.8 447588
280-127755-4 C 19081073-002C Dissolved Water 200.8 447588
280-127755-7 C 19081073-003C Dissolved Water 200.8 447588
280-127755-10 C 19081073-004C Dissolved Water 200.8 447588
280-127755-13 C 19081073-005C Dissolved Water 200.8 447588
280-127755-16 C 19081073-006C Dissolved Water 200.8 447588
280-127755-19 C19081073-007C Dissolved Water 200.8 447588
280-127755-22 C 19081073-008C Dissolved Water 200.8 447588
280-127755-25 M3-54865 Dissolved Water 200.8 447588
Eurofins TestAmerica, Denver
Page 20 of 31 Page 145 of 172
Lab Chronicle
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
ProjecUSite: 11 (e) Byproduct Material
Client Sample ID: C19081073-001C Lab Sample ID: 280-127755-1
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 200 7/200.8 34 ml 50 ml 447588 10/24/19 13:54 LAM TALSL
Dissolved Analysis 200.8 500 448112 10/29/1901 :25 FLC TALSL
Client Sample ID: C19081073-002C Lab Sample ID: 280-127755-4
Date Collected: 08/21/19 09:05 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 200.7/200.8 50ml 50 ml 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 50 447983 10/26/19 06:24 FLC TALSL
Dissolved Prep 200.7/200.8 50 ml 50 ml 447588 10/24/19 13:54 LAM TALSL m Dissolved Analysis 200.8 500 448112 10/29/19 01:31 FLC TALSL
Client Sample ID: C19081073-003C Lab Sample ID: 280-127755-7
Date Collected: 08/21/19 09:20 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 200.7/200.8 -5~ 50 ml 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 50 447983 10/26/19 06:31 FLC TAL SL
Dissolved Prep 200.7/200.8 50 ml 50 ml 447588 10/24/19 13:54 LAM TALSL
Dissolved Analysis 200.8 500 448112 10/29/19 01:38 FLC TALSL
Client Sample ID: C19081073-004C Lab Sample ID: 280-127755-10
Date Collected: 08/21/19 09:40 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Pre_p __ 200.7/200.8 50 ml 50 ml 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 50 447983 10/26/19 06:37 FLC TAL SL
Dissolved Prep 200.7/200.8 50 ml 50 ml 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 500 448112 10/29/1901 :45 FLC TAL SL
Client Sample ID: C19081073-005C Lab Sample ID: 280-127755-13
Date Collected: 08/21/19 09:45 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 200.7/200.8 35 ml 50 ml 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 50 447983 10/26/19 06:44 FLC TALSL
Dissolved Prep 200.7/200.8 35 ml 50 ml 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 500 448112 10/29/1901 :51 FLC TAL SL
Eurofins TestAmerica, Denver
Page 21 of 31 Page 146 of 172
Lab Chronicle
Client: Energy Laboratories, Inc. Job ID: 280-127755-2
Project/Site: 11 (e) Byproduct Material
Client Sample ID: C19081073-006C Lab Sample ID: 280-127755-16
Date Collected: 08/21/19 10:15 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Oil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 200.7/200.8 25 ml -50ml 447588 10/24/19 13:54 LAM TALSL-
Dissolved Analysis 200.8 50 447983 10/26/19 06:51 FLC TAL SL
Dissolved Prep 200.7/200.8 25 ml 50 ml 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 500 448112 10/29/19 01 :58 FLC TAL SL
Client Sample ID: C19081073-007C Lab Sample ID: 280-127755-19
Date Collected: 08/21/19 10:30 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Oil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 200.7/200.8 25 ml 50 ml 447588 10/24/19 13:54 LAM TALSL
Dissolved Analysis 200.8 50 447983 10/26/19 06:58 FLC TALSL
Dissolved Prep 200.7/200.8 25 ml 50 ml 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 500 448112 10/29/19 02:05 FLC TALSL
Client Sample ID: C19081073-008C Lab Sample ID: 280-127755-22
Date Collected: 08/21/19 08:35 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Oil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Dissolved Prep 200.7/200.8 10 ml 5~ 447588 10/24/19 13:54 LAM TALSL
Dissolved Analysis 200.8 50 447983 10/26/19 07:25 FLC TAL SL
Dissolved Prep 200.7/200.8 10 ml 50 ml 447588 10/24/19 13:54 LAM TALSL
Dissolved Analysis 200.8 500 448112 10/29/19 02:12 FLC TALSL
Client Sample ID: M3-54865 Lab Sample ID: 280-127755-25
Date Collected: 08/23/19 11 : 20 Matrix: Water
Date Received: 08/28/19 10:45
Batch Batch Oil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab -----Dissolved Prep 200.7/200.8 50ml 50ml 447588 10/24/19 13:54 LAM TAL SL
Dissolved Analysis 200.8 2 448112 10/29/19 02:18 FLC TAL SL
Laboratory References:
TAL SL= Eurofins Tes!America, St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL [phone]
Eurofins TestAmerica, Denver
Page 22 of 31 Page 147 of 172
Accreditation/Certification Summary
Client: Energy Laboratories, Inc.
Project/Site: 11 (e) Byproduct Material
Laboratory: Eurofins TestAmerica, Denver
Job ID: 280-127755-2
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
A2LA Dept. of Defense ELAP 2907.01 10-31-21
A2LA ISO/IEC 17025 2907.01 10-31-21
Alabama State Program 40730 09-30-12 *
Alaska (UST) State 18-001 01-08-20
Arizona State AZ0713 12-20-19
Arkansas DEQ State 19-047-0 06-01-20
California State 2513 01-08-20
Connecticut State PH-0686 09-30-20
Florida NELAP E87667-57 06-30-20
Georgia State 4025-011 01-08-20
Illinois NELAP 2000172019-1 04-30-20
Iowa State IA#370 12-01-20
Kansas NELAP E-10166 04-30-20
Louisiana NELAP 30785 06-30-20
Maine State 2019011 [phone]
Minnesota NELAP 1545373 12-31-19
Nevada State C0000262020-1 07-31-20
New Hampshire NELAP 205319 04-28-20
New Jersey NELAP 190002 06-30-20
New York NELAP 59923 04-01-20
North Carolina (WW/SW) State <cert No.> 12-31-19
North Dakota State R-034 01-08-20
Oregon NELAP 4025-011 01-08-20
Pennsylvania NELAP 013 08-01-20
South Carolina State 72002001 01-08-20
Texas NELAP T104704183-19-17 09-30-20
US Fish & Wildlife Federal 07-31-20
US Fish & Wildlife US Federal Programs 058448 07-31-20
USDA Federal 03-26-21
USDA US Federal Programs P330-18-00099 03-26-21
Utah NELAP C0000262019-11 07-31-20
Virginia NELAP 10490 06-14-20
Washington State C583-19 08-05-20
Wisconsin State 999615430 08-31-20
Wyoming (UST) A2LA 2907.01 10-31-21
* Accreditation/Certification renewal pending -accreditation/certification considered valid.
Eurofins TestAmerica, Denver
Page 23 of 31 Page 148 of 172
Accreditation/Certification Summary
Client: Energy Laboratories, Inc.
ProjecUSite: 11 (e) Byproduct Material
Laboratory: Eurofins TestAmerica, St. Louis
Job ID: 280-127755-2
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
ANAB Dept. of Defense ELAP L2305 04-06-22
ANAB Dept. of Energy L2305.01 04-06-22
ANAB ISO/IEC 17025 L2305 04-06-22
Arizona State AZ0813 12-08-19
California Los Angeles County Sanitation 10259 06-30-20
Districts
California State 2886 06-30-20
Connecticut State PH-0241 03-31-21
Florida NELAP E87689 06-30-20
HI -RadChem Recognition State n/a 06-30-20
Illinois NELAP 004553 11-30-19
Iowa State 373 09-17-20
Kentucky (OW) State KY90125 12-31-19
Louisiana NELAP 04080 06-30-20
Louisiana (OW) State LA011 12-31-19
Maryland State 310 09-30-20
Ml -RadChem Recognition State 9005 06-30-20
Missouri State 780 06-30-22
Nevada State M0000542020-1 07-31-20
New Jersey NELAP M0002 06-30-20
New York NELAP 11616 04-01-20
North Dakota State R-207 06-30-20
NRC NRC 24-24817-01 12-31-22
Oklahoma State 9997 08-31-20
Pennsylvania NELAP 68-00540 11-03-19
South Carolina State 85002001 06-30-20
Texas NELAP T104704193-19-13 07-31-20
US Fish & Wildlife US Federal Programs 058448 07-31-20
USDA US Federal Programs P330-17-00028 02-02-20
Utah NELAP M0000542019-11 07-31-20
Virginia NELAP 10310 06-14-20
Washington State C592 08-30-20
West Virginia DEP State 381 10-31-19
Eurofins TestAmerica, Denver
Page 24 of 31 Page 149 of 172
Energy Laboratories Inc Workorder Summary
Energy Fuels Resources (USA) Inc
Samp / Client Sample ID Collection Date Due Matrix Frac RT Done Test Code
T Analyte
C O O 200.7.8-W-D
111111111111111111111111111111111111111111111111111111
C19081073
Hold MS SEL Storage
MDL PQL MCL Units
D D 0 LG-2-000
OIOIOOfOOOOttoooooooooo,ooooo••••ooO•OOOoOoOOOOHOH O·OIOOOOOOOOOOOOOOIO••o••••••••••ooooooOOO>OoooOHOOIOOHIOOOOooOoo,o,1,n,oooooooOOOOOOIOOOOOOOOooooo,0000000000,HooOoloOOIOOOOoooo•••••••oo
A Arsenic 0.0001 0.001 0 ug/L
A Beryllium 0.0001 0.001 0 ug/L
A Cadmium 0.00005 0 001 0 ug/L
A Calcium 0.03 1 0
A Chromium 0.0005 0.005 0 ug/L
A Cobalt 0.00005 0.005 0 ug/L
A Copper 0.0001 0.005 0 ug/L
A Iron 0.001 0.02 0 ug/L
A Lead 0.00005 0.001 0 ug/L
A Magnesium 0.05 0
A Manganese 0.00005 0.001 0 ug/L
A Molybdenum 0.00005 0.001 0 ugll
A Nickel 0.0001 0 005 0 ug/L
A Potassium 0.0001 0
A Selenium 0.05 0.001 0 ug/L
A Silver 0.4 0.001 0 ug/L
A Sodium 0.0001 0
A Thallium 0.0005 0.0005 0 ug/L
A Tin 0.0004 0.05 0 ug/L
A Uranium 0.00002 0.0003 0 ugll
A Vanadium 0.0005 0.01 0 ug/L
A Zinc 0.001 0 u /L
Page 25 of 31 Page 150 of 172
"'1J Ill (0
Cl)
N en
0 -(,.)
....>.
lJ Ill (0
(D
~ ~
g,
~
--..J I\J
Energy Laboratories, Inc.
·2393 Salt Creek Hwy
Casper. WY &2601-9601
307.235.0515
Subcontractor.
Test America
4955 Yarrow St
Arvada. CO 80002
TEL: [phone]
FAX:
Acct #: 3037360100
Subcontractor's Client
C19081073-001C I
C19081073-001D [
C19081073-001F [
C19081073-002C ]
c 19081073-0020 I
C19081073-002F I
C1908107l-003C I
Aaueous
Aaueous
Aaueous
Aaueous
Aaueous
Aaueous
Aaueous
IUffillHli~~IHlllllll~I\I
C19081073
PO: ______ _
[ 08/21/1908:35A 11-250Ml-P-F-HN03
CHAIN-OF-CUSTODY RECORD
Earliest HT Expires: Wed, 8/28/2019 0835
Test Codes: SVOC-35IOC-8270 Earliest Due Date:
Page 1 of 3
23-Aug-19
9/27/2019
# Bus. Days Until Due: 24
R.e<iuested Tests
() "ti en en < i ::0 < < 0 "ti 0 0 () ± (") (") co I Cl l, 00 N
Cl ;.., "' N "' ;.., 0 -.J 0 ~ ? .:... ~ pl () ~ ::r: ~ 00 ,,
N ~ ....,
CJ 0
---~ ------------1 1 ----------------I 08/21/19 08:35 A 12 -1L-AG-NM-UP ---------------------D D DJ DJ D D D D D D D D D D D D
I 08/21/19 08:35 A 13-40Ml-CG-VOA-HCL --~---DDDDDJDDDDDDDDDDD
[ 08/21/19 09:05 A 11 -250ML-P-F-HN03 -----------[TI lJJ DD DD DD DD DD D DD D
-----------------00[I][I]0DDDDDDDDDDD I 08/21/1909:0SA 12-1L-AG-NM-UP
I 08/21119 09:05 A 13 -40ML.CG-VOA-HCL I -··---·--·,--·---·-·--,DDDD!JJDDDDDDDDDDD
. ··-· ·---·--·· .. ---···-·. ····--, lJJ [TIDD DD DD O ODD DD DD I 08/21/19 09:20 A l 1 -250ML-P-F-HN03
C19081073-003D I Aaueous l 08121119 09:20 A l2-1L-AG-NM-UP ---~--__.DD!JJ!JJDDDDDDDDDDDD
C 19081073-003F I Aaueous [ 08/21119 09:20 A 13-40ML-CG-VOA-HCL ------~DDDD!JJDDDQnDDDDOD
Comments:
QC Level:
11E(2)
~8Clf :57 8"
Date/fime
2s0-12n55 Chain of Custody ---
Date/fime-,?"
a,1;nqW,b•dby:(~+:1,<uL ~3 ,;g
Relinquished by: a .2t 5 Q
Received by: ~ 2 f :::::----,,,,, :> yzr£/1C, ~
Received by: I olf S
Shipped By: U ~ Custody Seal -.-.. y
Intact ......... N
Temp Blank yG2) On Ice G) N Receipt Temp: L .S-1 '7.<P,2;i
~
""O Q) (0 m
~ ~
0 -(,)
-"
"C "' <O <D
~
01 "' a
~
-..J "'
Ener2}' Laboratories, Inc.
·2393 Salt Creek Uwy
Casper, WY 82601-9601
307.235.0515
Subcontractor:
Test America
4955 Yarrow St
Arvada. CO 80002
TEL: [phone]
FAX:
Acct#: 3037360100
Subcontractor's Client
C 19081073-004C
C19081073-004D
C19081073-004F
C19081073-005C
C19081073-005D
C19081073-005F
Aaueous
Aaueous
AQueous
AQueous
Aaueous
Aaueous
PO: ______ _
08/21/19 09:40 A I 1 -250ML-P-F-HN03
CHAIN-OF-CUSTODY RECORD
Earliest HT Expires: Wed, 8/28/2019 0835
Test Codes: SVOC-3510C-8270 Earliest Due Date:
Page 2 of3
23-Aug-19
9/27/2015
# Bus. Days Until Due: 24
ReQuested Tests
(") "ll (/) (/) < ~ JJ < ~ 0 -0 0 c;> ± (") (") 00 ± 0 w &, "' 0 "' ~ N a,
"' 0 "' ti, 8 9 .:.. -I> ~ J: 01 ~ &, ~ "Tl N :E "' 0 0
,__ --'--L-f--,___ ,__ ,__ ,___ ,__ ,__ '----,___
1 1 ----,__ ..__ -----,__ ...... ,__ --
08121/19 09:40 A 12 -1 L-AG-NM-UP
08121/19 09:40 A I3-40ML-CG-VOA-HCL
________ oommoooooooooooo
--------------DD DD OJ DD DD DD DD DD D
08/21/19 09:45 A {1 -250ML-P-F-HN03 -·----.. -----.. -· ..... __ OJOJDDDDDDDDDDDDDD
08/21/19 09:45A 12 -1L-AG-NM-UP -------------------D D OJ OJ D D D D D D D D D D D D
08/21/19 09:45 A I 3 -40ML-CG-VOA-HCL -------------DDDDOJDDDDDDDDDDD
C19081073-006C Aqueous 08/21/19 10:15 A I 1 -250ML-P-F-HN03 ---------~mOJDDDDDDDDDDDDDD
C19081073-006D Aaueous 08/21/19 10:15 A f2 -1L-AG-NM-UP ---------·····-oommDDDDDDDDDDDD
C19081073-00SF AQueous j 08/21/1910:15A !3-40ML-CG-VOA-HCL -----~DDDDDJDDDDDDDDDDD
Comments:
QC Level:
11E(2)
Reeo;v,d by, ~ Z "') ~~!Time
Relinquished by: 'fr 1o 'i:i
Relinquished by: Received by:
Intact "2~ 7.& 7,f Temp Blank On Ice
Shipped By: uQ N Q)N Receipt Temp: -' 1 •c y C1b Cb N
~
"U
Ill (C
CD
N CX>
0 -w ....>.
"U Dl <O <D
~
(.11 c,.)
a
~
--J "'
Enerizy Laboratories, Inc.
2393 Salt Creek Hwy
Casper, WY 82601-960 I
307.235.0515
Subcontractor:
Test America
4955 Yarrow St
Arvada. CO 80002
TEL: [phone]
FAX:
Acct #: 3037360100
Subcontractor's Client
C19081073--007C I
C19081073-0070 I
C19081073-007F I
C 19081073--008C I
C19081073--008D I
C19081073-008F I
Comments:
Aaueous
Aaueous
Aaueous
Aaueous
Aaueous
Aaueous
PO:. ______ _
I 08/21119 10:30 A 11 -250ML-P-F-HN03
CHAIN-OF-CUSTODY RECORD
Earliest HT Expires: Wed, 8/28/2019 0835
Test Codes: SVOC-3510C-8270 Earliest Due Date:
Page 3 of 3
23-Aug-19
9/27/2019
# Bus. Days Until Due: 24
Reouested Tests
C) "tl en en < < ::0 < < 0 ~ "tl 0 0 (") :I: c;, <;l 00 I G) w C)O "" Cl ~ u, "" a,
~ 0 ...... 0 ~ ? -'-4 ~ !,71 (") ~ I U1 ~ 00 ~ ,,
"" ~ ......
C 0
.__ ---------------1 ....!.. ---------------I 08/21/1910:30 A j2-1L-AG-NM-UP
I 08/21/19 10:30 A 13 -40ML-CG-VOA-HCL
I 08/21119 08:35 A I 1 -250ML-P-F-HN03
I 1ooruruDDDDDDDDDDDD
1--···---·---IDDDDruDDDDDDDDDDD
--. -----I -------I ru ITl D D D D D D D D D DD D D D
I 08/21/19 08:35 A {2-1L-AG-NM-UP ---··------· 1--·-·····-IDDITJITJDDDDDDDDDDDD
I 08/21/19 08:35 A ~3 -40MI -I'-r.-vnA.Hr.1 -···---·--··1-·-···-----------IDDDDruDDDDDDDDDDD
QC Level:
11E(2)
rf}/!/ee-::;'-:} S {'I/ '1 :, 7~
~
Shipped By: \ )'<5
Date/Time Date/Time
Received by:~C:::-:--<{/z. ~/l'i lo'-/5
Received by?
C;istody Seal I J~~act ~ N (?; N
-------------
Receipt Temp: 2-. 5, ?. '7, ?$ ·c
ag
TempB~
y (_~'
,r-q_n Ice
L:£) N
"U
Dl <O (D
N CD
0 -,, w ......
"tl ~ (1)
i
Q, .....
-.J N
Eurofins TestAmerica, Denver
4955 Yarrow Street
Arvada. CO 80002
Phone: [phone] Fax: [phone]
Client Information {Sub Contract Lab)
Clienl Conlacl:
Shipping/Receiving
Company:
TestAmerica Laboratories. Inc.
Sompler:
Ptione:
Chain of Custody Record
Lab PM;
Vania. Ivan H
E·Mll~:
[e-mail]
Accr<Klffalions Requlr<KI (5ee nole):
111~11 !Hll 11!1111m111~111~~~rn~ 1mm, ;~:; e LI ro fj n s
Carner Tracking No(s):
State of Origin:
Wyoming
COCNo:
280-502172.1
Page:
Page 1 of 1
Job#:
280-127755-2
E.:1vin.•nmcn1 i1• ;'.11
ln.stAm':'rti':.'l
A&tress! Due Date Requested:
1·13715 Rider Trail North. , 10/28/2019 Analysis Requested A· HCL
Preservation Codes:
[City: TAT Requested (days): B -NaOH
Earth City C -Zn Acetale
Stale. Zip: 0 D -Nitric Acid
MO. 63045 ; ; : :~~o4
Phone: PO #: , lil G -Amchlor
314-298-8566(Tel) 314-298-8757(Fax) ti' !!1 H -Ascorbic Acid
Emal: WO#: ~ _ ~ I-Ice
~ ! g !! J-D1Water
... N ! K·EDTA Project Name: Projecl #: ~ 0 o -L _ EDA
11(e) Byproduct Material 28019578 Ji! I g i
Stte: SSOW#: f cl:. c g OCher:
M-Hexane
N-None
0-AsNa02
P-Na2045
O-Na2S03
R-Na2S203
S -H2S04
T. TSP Dodecahydrate
U-Acelone
V-MCAA
W -pH 4-5
Z -other (specify)
~1! ~. I i, .x·----------------1 ~m-M~• ~ g ~
Sample
Sample ldentificatlon -Client ID (Lab ID) Sample Date Time
Type <--···-~ I ~ ! (C=comp. o-.. waa. 1 . ~ I
G=grab) 9T.,,,. ......... 1 U:: , ::: 1-Special Instructions/Note:
-~ -PreSl!Milion Code: -><· ~ · 1X1
08:"35 C19081073-001C (280-127755-1) 8/21/19 Mountain Waler X
C19081073-002C (280-127755-4) 8/21/19 09:05
u,.., nt,.in Water X
C19081073-003C (280-127755-7) 8/21/19 09:20
Mno ntain Water X
C19081073-004C (280-127755-10) 8121/19 09:40
Mountain Water X
C19081073-005C (280-127755-13) 8/21/19 09:45
u""""'in Water X
C19081073-006C (280-127755-16) 8/21/19 10:15
Mn11nt,.in Water X
C19081073-007C (280-127755-19) 8/21/19 10:30
Mountain Water X
1C19081073-008C (280-127755-22) 8/21/19 08:35
u,.. .. n,,.in Water X
1M3-54865 (280-127755-25) 8/23/19 11:20
Mn.!.1!1lfiln Water X
Nol.e-Since labo<ato<y acaadilalloos are subject 10 change. Tes!Amerlca LaD0rat0t1SS. tnc:. plates Ille owoersnlp of ,nell1od. ahalyte & accre<11ta1,on cornpbanc,e uPQn out sut>conllact tal>oralonM. lh,s sample stilpment ,s fo,warded under chain-or-custody w tne laboratory does not
cuner>Uy maintal'I acuedillll!Cll'I In the Stato ClC Ong,n r.sted abOve for analr.;islleS!Simatri• being analyzed. lne ,sa,...pleS muSI oe sh,ppeo bat~ lo ll\e Tes1A1!1etic;a lal>OfalOl)'o< olller in~ucllo,,s wiG be provided. Any changes lo accred1lahon slalus should be brought 10 TestAmenca
labOralO(les, Int, alttlf1tion mmediatety. tt-.,~ requesleO accn,dfta11ons are curTent lO elate, rewrn 1t11, sl9fled Chain of Cuslody artesting 10 said comp,cance 10 TeslAmeric:a Labor.ilcries. lt1e.
Possible Hazard Identification
Level 1 radioactive
Deliverable Requested: I. II. Ill. IV, Other (specify)
Empty Kn R~quished by:
Re~Ulshed DY: ~ -~7
~ 7'
Renfl'l'tShec1 Dy:..._
Ro6t>Qul:llled by:
Custody Seals lntacl: 'Custody Seal No.:
6 Yes ,\ No
Primary Deliverable Rank: 2
1Date:
0&?7if.Pf f I '-I~
Dale!l'ime: I
Datemme:
Sample Disposal ( A fee may be assessed if samples are retained longer than 1 month)
D Re tum To Client D Disposal _Br Lab D Archive For Months
Special Instructions/QC Requirements:
1nme:
Company :.....:..:.H!:t --:AJIReceiv<KI by: -, rr~O ~.e'-
Company Received by:
Company Received by:
MelMod or Shipment
DaWTf"e. I ihll-7-1LJ
Dale/Time:
Datemme:
Cooler Temperature(s) "C and Olher Remarks.
~
Oy~SS Company rAS f L
Company
Company
Ver: 01116120!9
Login Sample Receipt Checklist
Client: Energy Laboratories, Inc.
Login Number: 127755
List Number: 1
Creator: Petunin, Peter
Job Number: 280-127755-2
List Source: Eurofins TestAmerica, Denver
Question Answer Comment
Radio activity wasn't checked or is </= background as measured by a survey True
meter.
The cooler's custody seal, if present, is intact. True
Sample custody seals, if present, are intact. True
The cooler or samples do not appear to have been compromised or True
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
True
False
True
True
True
True
True
There are no discrepancies between the containers received and the COC. False
Samples are received within Holding Time (excluding tests with immediate True
HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
Eurofins TestAmerica, Denver
Page 30 of 31
--------------------
Cooler temperature outside required temperature
criteria.
Refer to Job Narrative for details.
Page 155 of 172
Login Sample Receipt Checklist
Client: Energy Laboratories, Inc.
Login Number: 127755
List Number: 2
Creator: McKinney, Gerrod E
Question
Radioactivity wasn't checked or is </= background as measured by a survey
meter.
The cooler's custody seal, if present, is intact.
Sample custody seals, if present, are intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no discrepancies between the containers received and the COC.
Samples are received within Holding Time (excluding tests with immediate
HTs)
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Residual Chlorine Checked.
Eurofins TestAmerica, Denver
Answer
True
True
N/A
True
True
True
True
True
True
True
N/A
True
True
True
True
True
True
True
True
True
N/A
N/A
True
N/A
Page 31 of 31
Job Number: 280-127755-2
List Source: Eurofins TestAmerlca, St. Louis
List Creation: 10/21/19 01:47 PM
Comment
Page 156 of 172
EN:RGY
' ' '
Trust our People. Trust our Data.
www.energylab.com
QA/QC Summary Report
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686. 7175 • Helena, MT 877.472.0711
Client: Energy Fuels Resources (USA) Inc
Prepared by Casper, WY Branch
Work Order: C19081073 Report Date: 09/19/19
Analyte
Method: A2320 B
Lab ID: ICV
pH
Method: A2320 B
Lab ID: MBLK
Alkalinity, Total as CaC03
Lab ID: LCS
Alkalinity, Total as CaC03
Lab ID: C19081073-00SADUP
Alkalinity, Total as CaC03
Qualifiers:
RL -Analyte reporting limit.
Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual
Initial Calibration Verification Standard
Analytical Run: MANTECH_ 190823A
08/23/19 09:38
102 6.91 s.u. 0.010 101 98
Batch: R250228
Method Blank Run : MANTECH_ 190823A 08/23/19 15:48
ND mg/L 2
Laboratory Control Sample Run: MANTECH_ 190823A 08/23/19 15:56
253 mg/L 5.0 101 90 110
Sample Duplicate Run: MANTECH_190823A 08/23/19 16:02
ND mg/L 5.0 10
ND -Not detected at the reporting limit.
Page 157 of 172
EN:RGY Trust our People. Trust our Data.
www.energylab.com
QA/QC Summary Report
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
Client: Energy Fuels Resources (USA) Inc
Prepared by Casper, WY Branch
Work Order: C19081073 Report Date: 09/19/19
Analyte
Method: A2510 B
Lab ID: SC 100
Conductivity @ 25 C
Lab ID: SC 5000
Conductivity @ 25 C
Lab ID: SC 20000
Conductivity @ 25 C
Method:
Lab ID:
A2510 B
SC 50000
Conductivity @ 25 C
Lab ID: MBLK
Conductivity @ 25 C
Lab ID: C190B1073-002ADUP
Conductivity @ 25 C
Qualifiers:
RL -Analyte reporting limit.
Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual
Analytical Run: PHSC_ 101-C_ 190823A
Initial Calibration Verification Standard
99.0 umhos/cm 5.0 99 90 110
Initial Calibration Verification Standard
4930 umhos/cm 5.0 99 90 110
Initial Calibration Verification Standard
20100 umhos/cm 5.0 101 90 110
Initial Calibration Verification Standard Run: PHSC_101-C_190823A
49700 umhos/cm 5.0 99 90 110
Method Blank Run: PHSC_101-C_190823A
0.5 umhos/cm
Sample Duplicate Run: PHSC_101-C_190823A
55700 umhos/cm 5.0
ND -Not detected at the reporting limit.
0.0
08/23/19 09:11
08/23/19 09:15
08/23/19 09:17
Batch: R250189
08/23/19 09:20
08/23/19 10:56
08/23/19 11 :37
10
Page 158 of 172
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Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877 .472.0711
QA/QC Summary Report
Client: Energy Fuels Resources (USA) Inc
Prepared by Casper, WY Branch
Work Order: C19081073 Report Date: 09/19/19
Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual
Method: A2540 C Batch: TDS190823A
Lab ID: MB-25_ 190823A Method Blank Run: ORG_BAL3_C_190823A 08/23/19 14:00
Solids, Total Dissolved TDS @ 180 C 1.0 mg/L
Lab ID: LCS-26_ 190823A Laboratory Control Sample Run: ORG_BAL3_C_190823A 08/23/19 14:00
Solids, Total Dissolved TDS@ 180 C 1010 mg/L 10 101 90 110
Lab ID: C19081058-003A DUP Sample Duplicate Run: ORG_BAL3_C_190823A 08/23/19 14:01
Solids, Total Dissolved TDS@ 180 C 624 mg/L 10 0.7 5
Method: A2540 C Batch: TDS190826A
Lab ID: MB-1_190826A Method Blank Run: ORG_BAL3_C_ 190826A 08/26/19 15:22
Solids, Total Dissolved TDS@ 180 C 2 mg/L
Lab ID: LCS-2_ 190826A Laboratory Control Sample Run: ORG_BAL3_C_190826A 08/26/19 15:23
Solids, Total Dissolved TDS@ 180 C 1000 mg/L 10 100 90 110
Lab ID: C19080975-002B DUP Sample Duplicate Run: ORG_BAL3_C_190826A 08/26/19 15:24
Solids, Total Dissolved TDS @ 180 C 181 mg/L 10 0.4 5
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
Page 159 of 172
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Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686. 7175 • Helena, MT 877.472.0711
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Work Order: C19081073 Report Date: 09/19/19
Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual
Method: A4500-F C Batch: R250269
Lab ID: LCS Laboratory Control Sample Run: MANTECH_ 190826A 08/26/19 17:18
Fluoride 2.12 mg/L 0.10 106 90 110
Lab ID: MBLK Method Blank Run: MANTECH_ 190826A 08/26/19 17:22
Fluoride ND mg/L 0.02
Lab ID: C19081073-004AMS Sample Matrix Spike Run: MANTECH_190826A 08/26/19 18:39
Fluoride 1850 mg/L 51 20 90 110 s
Lab ID: C19081073-005ADUP Sample Duplicate Run: MANTECH_ 190826A 08/26/19 18:47
Fluoride 1480 mg/L 50 3.7 10
Method: A4500-F C Batch: R250918
Lab ID: LCS Laboratory Control Sample Run: MANTECH_ 190913A 09/13/19 13:26
Fluoride 1.96 mg/L 0.10 98 90 110
Lab ID: MBLK Method Blank Run: MANTECH_ 190913A 09/13/19 13:31
Fluoride ND mg/L 0.02
Lab ID: C19090430-001AMS Sample Matrix Spike Run: MANTECH_ 190913A 09/13/19 13:47
Fluoride 2.16 mg/L 0.10 101 90 110
Lab ID: C19090430-002ADUP Sample Duplicate Run: MANTECH -190913A 09/13/19 13:53
Fluoride 0.180 mg/L 0.10 5.4 10
Method: A4500-F C Batch: R251103
Lab ID: LCS Laboratory Control Sample Run: MANTECH_ 190918A 09/18/19 13:47
Fluoride 1.89 mg/L 0.10 94 90 110
Lab ID: MBLK Method Blank Run: MANTECH_ 190918A 09/18/19 13:52
Fluoride ND mg/L 0.02
Lab ID: C19090613-001AMS Sample Matrix Spike Run: MANTECH_ 19091 BA 09/18/19 14:11
Fluoride 2.00 mg/L 0.10 86 90 110 s
Lab ID: C19090613-002ADUP Sample Duplicate Run: MANTECH_ 190918A 09/18/1914:16
Fluoride 0.430 mg/L 0.10 0.0 10
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
Page 160 of 172
EN:RGY Trust our People. Trust our Data.
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QA/QC Summary Report
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 886.686.7175 • Helena, MT 877.472.0711
Client: Energy Fuels Resources (USA) Inc
Prepared by Casper, WY Branch
Work Order: C19081073 Report Date: 09/19/19
Analyte
Method: A4500-H B
Lab ID: 6.86
pH
pH Measurement Temp
Method: A4500-H B
Lab ID: C19081073-002ADUP
pH
pH Measurement Temp
Qualifiers:
RL -Analyte reporting limit.
Count Result Units RL %REC Low Limit High Limit RPO RPDLimit Qual
2 Initial Calibration Verification Standard
Analytical Run: PHSC_101-C_190823A
08/23/19 09:08
102 6.87 s.u.
19.4 ·c
2 Sample Duplicate
3.07 s.u.
16.6 ·c
0.010 100
0.010
98
0 0
Run: PHSC_ 101-C_ 190823A
ND -Not detected at the reporting limit.
0.0
Batch: R250189
08/23/19 11 :37
1.5
Page 161 of 172
EN:RGY Trust our People. Trust our Data.
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Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 886.686. 7175 • Helena, MT 877.472.0711
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Work Order: C19081073 Report Date: 09/19/19
Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual
Method: E300.0 Analytical Run: IC3-C_ 190909A
Lab ID: ICV 2 Initial Calibration Verification Standard 09/09/19 17:02
Chloride 9.82 mg/L 1.0 98 90 110
Sulfate 38.7 mg/L 1.0 97 90 110
Method: E300.0 Batch: R250799
Lab ID: ICB 2 Method Blank Run: IC3-C_ 190909A 09/09/19 17:21
Chloride ND mg/L 0.05
Sulfate 0.2 mg/L 0.1
Lab ID: LFB 2 Laboratory Fortified Blank Run: IC3-C_ 190909A 09/09/19 17:41
Chloride 9.86 mg/L 1.0 99 90 110
Sulfate 38.7 mg/L 1.0 97 90 110
Lab ID: C19090268-001AMS 2 Sample Matrix Spike Run: IC3-C -190909A 09/10/19 11 : 16
Chloride 16.4 mg/L 1.0 103 80 120
Sulfate 55.8 mg/L 1.0 101 80 120
Lab ID: C19090268-001 AMS D 2 Sample Matrix Spike Duplicate Run: IC3-C_ 190909A 09/10/1912:14
Chloride 16.3 mg/L 1.0 103 80 120 0.4 20
Sulfate 55.7 mg/L 1.0 101 80 120 0.2 20
Method: E300.0 Analytical Run: IC3-C_ 190912A
Lab ID: ICV 2 Initial Calibration Verification Standard 09/12/19 11 :59
Chloride 9.87 mg/L 1.0 99 90 110
Sulfate 39.0 mg/L 1.0 97 90 110
Method: E300.0 Batch: R250929
Lab ID: ICB 2 Method Blank Run: IC3-C_190912A 09/12/19 12:18
Chloride ND mg/L 0.05
Sulfate 0.2 mg/L 0.1
Lab ID: LFB 2 Laboratory Fortified Blank Run: IC3-C_190912A 09/12/19 12:37
Chloride 9.97 mg/L 1.0 100 90 110
Sulfate 39.1 mg/L 1.0 98 90 110
Lab ID: C19090430-001AMS 2 Sample Matrix Spike Run: IC3-C_ 190912A 09/13/19 20:55
Chloride 26.3 mg/L 1.0 103 80 120
Sulfate 266 mg/L 1.0 99 80 120
Lab ID: C19090430-001 AMSD 2 Sample Matrix Spike Duplicate Run: IC3-C_190912A 09/13/1921 :15
Chloride 26.3 mg/L 1.0 103 80 120 0.1 20
Sulfate 266 mg/L 1.0 100 80 120 0.2 20
Qualifiers:
RL -Analyte reporting limit. ND -Not detected at the reporting limit.
Page 162 of 172
EN:RGY
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www.energylab.com
Billings, MT 800.735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
QA/QC Summary Report
Client: Energy Fuels Resources (USA) Inc
Prepared by Casper, WY Branch
Work Order: C19081073 Report Date: 09/19/19
Analyte
Method: E350.1
Lab ID: ICV
Nitrogen, Ammonia as N
Method: E350.1
Lab ID: MBLK
Nitrogen, Ammonia as N
Lab ID: LFB
Nitrogen, Ammonia as N
Lab ID: C19081073-00SBMS
Nitrogen, Ammonia as N
Lab ID: C19081073-00SBMSD
Nitrogen, Ammonia as N
Qualifiers:
RL -Analyte reporting limit.
Count Result Units RL %REC Low Limit High Limit RPO RPDLimit Qual
Initial Calibration Verification Standard
0.996 mg/L 0.050
Method Blank
ND mg/L 0.03
Laboratory Fortified Blank
0.941 mg/L 0.050
Sample Matrix Spike
30000 mg/L 1300
Sample Matrix Spike Duplicate
30800 mg/L 1300
100
95
96
99
90
Analytical Run: FIA201-C_1908268
08/26/1917:15
110
Batch: R250266
Run: FIA201-C_1908268 08/26/19 17: 14
Run: FIA201-C_1908268 08/26/19 17:16
90 110
Run: FIA201-C_1908268 08/26/19 18:11
90 110
Run: FIA201-C_ 1908268 08/26/19 18:13
90 110 2.5 10
ND -Not detected at the reporting limit.
Page 163 of 172
EN:RGY
' ' '
Trust our People. Trust our Data.
www.energylab.com
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686 . 7175 • Helena , MT 877.472.0711
QA/QC Summary Report
Client: Energy Fuels Resources (USA) Inc
Prepared by Casper, WY Branch
Work Order: C19081073 Report Date: 09/19/19
Analyte
Method: E353.2
Lab ID: ICV
Nitrogen, Nitrate+Nitrite as N
Method: E353.2
Lab ID: MBLK
Nitrogen, Nitrate+Nitrite as N
Lab ID: LFB
Nitrogen, Nitrate+Nitrite as N
Lab ID: C19081063-004AMS
Nitrogen, Nitrate+Nitrite as N
Lab ID: C19081063-004AMSD
Nitrogen, Nitrate+Nitrite as N
Qualifiers:
RL -Analyte reporting limit.
Count Result Units RL %REC Low Limit High Limit RPO RPDLlmit Qual
Initial Calibration Verification Standard
1.04 mg/L 0.010
Method Blank
ND mg/L 0.010
Laboratory Fortified Blank
0.951 mg/L 0.010
Sample Matrix Spike
1.68 mg/L 0.010
Sample Matrix Spike Duplicate
1.69 mg/L 0.010
104
96
98
99
90
Analytical Run: FIA201-C_190827A
08/27 /19 11 :30
110
Batch: R250300
Run: FIA201-C_190827A 08/27/1911:32
Run: FIA201-C_ 190827A 08/27 /19 11 :33
90 110
Run: FIA201-C_190827A 08/27 /19 11 :53
90 110
Run: FIA201-C_190827A 08/27 /19 11 :54
90 110 0.6 10
ND -Not detected at the reporting limit.
Page 164 of 172
EN:RGY ~~ Trust our People. Trust our Data.
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Work Order Receipt Checklist
Energy Fuels Resources (USA) Inc
Login completed by: Casie C. Peppersack
Reviewed by: Kasey Vidick
Reviewed Date: 8/26/2019
Shipping container/cooler in good condition?
Custody seals intact on all shipping container(s)/cooler(s)?
Custody seals intact on all sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
(Exclude analyses that are considered field parameters
such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.)
Temp Blank received in all shipping container(s)/cooler(s)?
Container/Temp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Standard Reporting Procedures:
Yes 0
Yes D
Yes D
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
0.0°C On Ice
Yes 0
Yes D
Billings, MT 800. 735.4489 • Casper, WY 888.235.0515
Gillette, WY 866.686.7175 • Helena, MT 877.472.0711
C19081073
Date Received: 8/22/2019
Received by: ens
Carrier name: Hand Del
No D
No D
No D
No D
No D
No D
No D
No D
No D
No D
No D
No D
No D
Not Present D
Not Present 0
Not Present 0
Not Applicable D
No VOA vials submitted D
Not Applicable 0
Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as
pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time.
Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected,
data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried
and ground prior to sample analysis.
Contact and Corrective Action Comments:
Additional temperatures 0.3, 4.0, 25.3, 27.0. Headspace noted on check list of which vials have headspace. 8/22/19
CP
Page 165 of 172
ENERGY -~ Chain of Custody & Analytical Request Record
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A, lnf1 ti R --. -~ ---.-------------------r· -·----------------------·---------·--·,
Company/Name Energy FUels Company/Name Energy Fuels
Contact Kathy Weinel Contact Tanner Holliday
Phone [phone] Phone [phone]
MaUing Address 225 Union Blvd, Suite 600 Mailing Address PO Box 809
City, State, Zip Lakewood, CO 80228 City, State, Zip Blanding, Utah 84511
Email [e-mail] Email [e-mail]
Receive Invoice CHard Copy aEmail I Receive Report CHard Copy •email Receive Report DHard Copy aemail
Purchase Ortlef lauote rottleOrder Special Repo<I/Formats:
C5645 Cl LEVEL IV D NElAC D EDD/EDT (oonrac:t laboratory) C Other STD EFRI
Project Information Matrix Codes Analysis Requested
Project Name, PWSID, Permit, etc. Annual Tails 2019 A-Air
W-Water
Sampler Name Tanner Holliday Sampler Phone [phone] S-Soils/ Solids
Sample Origin State Utah EPA/State Compliance a Yes CJ No V • Vogolatlc"
URANIUM MINING CLIENTS MUST Indicate sample type. B • Bioessay
0-other D NOT Source or Byproduct Material I() D Source/Processed Ore (Ground or Refined) .. CALL BEFORE SENDING r:,{'(. Dotnkl"g "S Waler
• 11e.(2) Bvoroduct Material (Can ONLY be Submitted to ELI ca-r Location) I() u
Sample Identification Collection Matrix !!
'Numberot 0
Containers ~Co-:::, (Name, Location, /nleMJJ, etc./ Date Time -· 0
1 Cell 1 8/21/19 011.~"C;, 11 0 X
2 Cell 2 Slimes 8/21/19 o~o~ 11 0 X
3 Cell 3 8/21/19 ()Cl.;t0 11 0 X
4 Cell 4A 8/21/19 O'PiO 11 0 X
s Cell 4ALDS 8/21/19 :'fl Lt.~ 11 0 X
a Cell 48 8/21/19 1015 11 0 X
1 Cell 48 LDS 8/21/19 103(} 11 0 X
e Cell 65 8/21/19 o~r~s 11 0 X
9
10
Custody
be signed
$hipped By Cooler ID{s) Payment Type
Cash Check.~~~~
Page_1~_of_1~-
Comments
Samples HAVE NOT BEEN
FILTERED
All tumaround times are
standard unless marked as
RUSH.
Energy Laboratories
MUST be contacted prior to ,, RUSH sample submittal for CII charges and scheduling -.c t) See Instructions Page 1111 = • <C a, R.?.t CII Ell LAB ID en TAT l..sbolalwy Use Only
!'/CJ{)'if J /) f ·-3 -·
In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All subcontracted data will be clearly notated on your analytical report. ru-coc-10/18 v.3
N r-
~
0
(0 (0
~
Ql Cl ra a.
EN:RGY [--------·--·-·-···-·---·---·--·-··--Trust our People. Trust our Data. Bi11ln1s, MT ID0.735.4419 • Casper, WY 181.235.8515
~w~ energy~.:_l>.~m • _ • . GIiiett,, WY IBI.Bll.1175 • Helena, MT 171.472.DJl 1
Energy Fuels Resources (USA) Inc
225 Union Blvd Ste 600
Lakewood, CO 80228-1826
Analytical Quote
Quote #: C5645
Project Manager: Tessa Parke
Expires: 8/11/2020
TAT: 25 days
QC Level: STD
Project Name: Annual Tailings Program
Schedule: Annual Tailings Samples
Comments:
Matrix: Aqueous
Analyses Method Reporting Limit Analyte Price
Alkalinity
Alkallnity, Total as caco3 A2320 B
Bicarbonate as HC03 A2320 B
Carbonate as C03 A2320 B
** Included In Alkalinity Price
Anions by Ion Chromatography
Chloride E300.0
Sulfate E300.0
** Included In Anions by Ion Chromatography Price
Fluoride
Fluoride A4500-F C
** Included In Fluoride Price
Metals by ICP/ICPMS, Dissolved
Calcium E200.7_8
Magnesium E200.7_8
Potassium E200.7_8
Sodium E200.7_8
** Included In Metals by ICP/ICPMS, Dissolved Price
Phplc:al ~
Conductivity
Conductivity @ 25 C
** Induded In Conductivity Price
pH
pH
A2510 B
A4500-H B
$10.00
5 mg/L **
5 mg/L **
5 mg/L **
$20.00
1 mg/L **
1 mg/L **
$15.00
0.1 mg/L **
$220.00
1 mg/L **
1 mg/L **
1 mg/L **
1 mg/L **
· .. ~ .·
$10.00
5 umhos/cm **
$10.00
0.01 s.u. **
Page 1
Page 161_-Ct~l ?~2~--
pH Measurement Temp A4500-H B 0 °C **
** Included in pH Price
Solids, Total Dissolved $20.00
Sollds, Tot.al Dissolved TDS @ A2540 C 10 mg/L **
180 C
** Included in Solids, Total Dissolved Price
Nutrlalta
Nitrogen, Ammonia $30.00
Nitrogen, Ammonia as N E350.1 0.05 mg/L **
** Included in Nitrogen, Ammonia Price
Nitrogen, Nitrate + Nitrite $50.00
Nitrogen, Nitrate+Nltrite as N E353.2 0.01 mg/L **
** Included in Nitrogen, Nitrate + Nitrite Price
Metala,·Dl•i;ilved
Mercury, Dissolved $25.00
Mercury E245.1 0.0001 mg/L **
** Included in Mercury, Dissolved Price
Metals by ICP/ICPMS, Dissolved ''""
Arsenic E200.7_8 1 ug/L **
Beryllium · E200.7_8 1 ug/L **
cadmium E200.7_8 1 ug/L **
Chromium E200.7_8 5 ug/L **
Cobalt E200.7_8 5 ug/L **
Copper E200.7_8 5 ug/L **
Iron E200.7_8 20 ug/L **
Lead E200.7_8 1 ug/L **
Manganese E200.7_8 1 ug/L **
Molybdenum E200.7_8 1 ug/L **
Nickel E200.7_8 5 ug/L **
Selenium E200.7_8 1 ug/L **
Silver E200.7_8 1 ug/L **
Thallium E200.7_8 0.5 ug/L **
lln E200.7_8 50 ug/L **
Uranium E200.7_8 0.3 ug/L **
Vanadium E200.7_8 10 ug/L **
Zinc E200.7_8 10 ug/L **
** Included in Metals by ICP/ICPMS, Dissolved Price
--Included In Major Ions Metals by ICP/ICPMS, Dissolved Price
Data Quallty
Anion -cation Balance A1030 E -250.01 $0.00
Solids, Total Dissolved -calculated A1030 E -250.01 mg/L $0.00
Volatile Olganlc Compounds
Page2
L---' IV VI -' -8260-Volatile Organic Compounds-$250.00
Extended List
1, 1, 1,2-Tetrachloroethane SW82608 1 ug/L **
1, 1, 1-Trlchloroethane SW8260B 1 ug/L **
1,1,2,2-Tetrachloroethane SW82608 1 ug/L **
1,1,2-Trichloroethane SW8260B 1 ug/L **
1, 1-Dld'lloroethane SW8260B 1 ug/L **
1, 1-Dlchloroethene SW8260B 1 ug/L **
1, 1-Dlchloropropene SW82608 1 ug/L **
1,2,3-Trlchlorobenzene SW8260B 1 ug/L **
1,2,3-Trlchloropropane SW8260B 1 ug/L **
1,2,4-Trichlorobenzene SW8260B 1 ug/L **
1,2,4-Trimethylbenzene SW8260B 1 ug/L **
1,2-Dlbromo-3-chloropropane SW8260B 1 ug/L **
1,2-Dibromoethane SW8260B 1 ug/L **
1,2-Dlchlorobenzene SW8260B 1 ug/L **
1,2-Dichloroethane SW8260B 1 ug/L **
1,2-Dichloropropane SW8260B 1 ug/L **
1,3,5-Trimethylbenzene SW8260B 1 ug/L **
1,3-Dichlorobenzene SW8260B 1 ug/L **
1,3-Dichloropropane SW8260B 1 ug/L **
1,4-Dlchlorobenzene SW8260B 1 ug/L **
2,2-Dlchloropropane SW8260B 1 ug/L **
2-Chloroethyl vinyl ether SW8260B 1 ug/L **
2-0'llorotoluene SW8260B 1 ug/L **
2-Hexanone SW8260B 20 ug/L **
4-Chlorotoluene SW8260B 1 ug/L **
Acetone SW8260B 20 ug/L **
Acetonltrlle SW82608 20 ug/L **
Acrolein SW8260B 20 ug/L **
Acrylonltrile SW8260B 20 ug/L **
Benzene SW8260B 1 ug/L **
Bromobenzene SW8260B 1 ug/L **
Bromochloromethane SW8260B 1 ug/L **
Bromodlchloromethane SW8260B 1 ug/L **
Bromoform SW8260B 1 ug/L **
Bromomethane SW8260B 1 ug/L **
carbon disulfide SW8260B 1 ug/L **
carbon tetrachloride SW8260B 1 ug/L **
Chlorobenzene SW8260B 1 ug/L **
Chlorodibromomethane SW8260B 1 ug/L **
Chloroethane SW8260B 1 ug/L **
Chloroform SW8260B 1 ug/l **
Chloromethane SW8260B 1 ug/L **
cis-1,2-Dlchloroethene SW8260B 1 ug/L **
cls-1,3-Dlchloropropene SW82608 1 ug/L **
Dibromomethane SW8260B 1 ug/L **
Dichlorodlfluoromethane SW8260B 1 ug/L **
Ethyl benzene SW8260B 1 ug/L **
Hexachlorobutadlene SW8260B 1 ug/L **
Iodomethane SW82608 1 ug/L **
Page 3
Page 169 of 172
Isopropylbenzene SW8260B 1 ug/L **
m+p-Xylenes SW8260B 1 ug/L **
Methyl ethyl ketone SW8260B 20 ug/L **
Methyl isobutyl ketone SW8260B 20 ug/L **
Methyl tert-butyl ether SW8260B 1 ug/L **
{MTBE) .
Methylene chloride SW8260B 1 ug/L **
Naphthalene SW8260B 1 ug/L **
n-Butylbenzene SW8260B 1 ug/L **
n-Propylbenzene SW8260B 1 ug/L **
o-Xylene SW8260B 1 ug/L **
p-Isopropyltotuene SW8260B 1 ug/L **
sec-Butylbenzene SW8260B 1 ug/L **
Styrene SW8260B 1 ug/L **
tert-Butylbenzene SW8260B 1 ug/L **
Tetrachloroethene SW8260B 1 ug/L **
Toluene SW8260B 1 ug/L **
trans-1,2-Dichloroethene SW8260B 1 ug/L **
trans-1,3-Dichloropropene SW8260B 1 ug/L **
Trichloroethene SW8260B 1 ug/L **
Trlchlorotluoromethane SW8260B 1 ug/L **
Vinyl acetate SW82608 1 ug/L **
Vinyl chloride SW8260B 1 ug/L **
Xylenes, Total SW8260B 0 ug/L **
** Included In 8260-Volatile Organic Compounds-Extended List Price
8260-Volatlle Organic Compounds-$130.00
Short List
Tetrahydrofuran SW8260B 10 ug/L **
** Included In 8260-Volatile Organic Compounds-Short List Price
.~Ql--,C~
Semi-Volatile Organic Compounds $350.00
1,2,4-Trichlorobenzene SW8270C 10 ug/L **
1,2-Dichlorobenzene SW8270C 10 ug/L **
1,3-Dlchlorobenzene SW8270C 10 ug/L **
1,4-Dlchlorobenzene SW8270C 10 ug/L **
1-Methylnaphthalene SW8270C 10 ug/L **
2,4,5-Trichlorophenol SW8270C 10 ug/L **
2,4,6-Trichlorophenol SW8270C 10 ug/L **
2,4-Dichlorophenol SW8270C 10 ug/L **
2,4-Dlmethylphenol SW8270C 10 ug/L **
2,4-Dinltrophenol SW8270C 50 ug/L **
2,4-Dinitrotoluene SW8270C 10 ug/L **
2,6-Dlnltrotoluene SW8270C 10 ug/L **
2-Chloronaphthalene SW8270C 10 ug/L **
2-Chlorophenol SW8270C 10 ug/L **
2-Methylnaphthalene SW8270C 10 ug/L **
2-Nitrophenol SW8270C 10 ug/L **
3,3 '-Dlchlorobenzldine SW8270C 10 ug/L **
4,6-Dinitro-2-methylphenol SW8270C 50 ug/L **
Page4
Page 170 at 172
4-Bromophenyl phenyl ether SW8270C 10 ug/L **
4-Chloro-3-methylphenol SW8270C 10 ug/L **
4-Chlorophenol SW8270C 10 ug/L **
4-Chlorophenyl phenyl ether SW8270C 10 ug/L **
4-Nitrophenol SW8270C 50 ug/L **
Acenaphthene SW8270C 10 ug/L **
Acenaphthylene SW8270C 10 ug/L **
Anthracene SW8270C 10 ug/L **
Azobenzene SW8270C 10 ug/L **
Benzidine SW8270C 10 ug/L **
Benzo(a)anthracene SW8270C 10 ug/L **
Benzo(a)pyrene SW8270C 10 ug/L **
Benzo(b )fluoranthene SW8270C 10 ug/L **
Benzo(g,h,i)perylene SW8270C 10 ug/L **
Benzo(k)fluoranthene SW8270C 10 ug/L **
bis(-2-chloroethoxy)Methane SW8270C 10 ug/L **
bis(-2-chloroethyl)Ether SW8270C 10 ug/L **
bis(2-chloroisopropyl)Ether SW8270C 10 ug/L **
bis(2-ethylhexyl)Phthalate SW8270C 10 ug/L **
Butylbenzylphthalate SW8270C 10 ug/L **
Chrysene SW8270C 10 ug/L **
Dibenzo( a,h)anthracene SW8270C 10 ug/L **
Diethyl phthalate SW8270C 10 ug/L **
Dimethyl phthalate SW8270C 10 ug/L **
Di-n-butyl phthalate SW8270C 10 ug/L **
Di-n-octyl phthalate SW8270C 10 ug/L **
Fluoranthene SW8270C 10 ug/L **
Fluorene SW8270C 10 ug/L **
Hexachlorobenzene SW8270C 10 ug/L **
Hexachlorobutadiene SW8270C 10 ug/L **
Hexachlorocyclopentadiene SW8270C 10 ug/L **
Hexachloroethane SW8270C 10 ug/L **
Indeno( 1,2,3-cd)pyrene SW8270C 10 ug/L **
Isophorone SW8270C 10 ug/L **
m+p-Cresols SW8270C 10 ug/L **
Naphthalene SW8270C 10 ug/L **
Nitrobenzene SW8270C 10 ug/L **
n-Nitrosodimethylamine SW8270C 10 ug/L **
n-Nitroso-di-n-propylamine SW8270C 10 ug/L **
n-Nitrosodiphenylamine SW8270C 10 ug/L **
o-Cresol SW8270C 10 ug/L **
Pentachlorophenol SW8270C SO ug/L **
Phenanthrene SW8270C 10 ug/L **
Phenol SW8270C 10 ug/L **
Pyrene SW8270C 10 ug/L **
Pyridine SW8270C 10 ug/L **
** Included in Semi-Volatile Organic Compounds Price
Prwpa For Annu .. TalUlffl• Samples
Pag~5
Page 171 of 172
Digestion, Mercury by OIAA E245.1
Sample Filtering, Metals
Separatory Funnel Liquid-Liquid Ext. SW3510C
Schedule Price/Sample:
Annual Tailings Samples
Quote Sub Total:
Discount:
Misc Charges:
Quote Total:
$0.00
$20.00
$0.00
$1160.00
$1160.00
$1160.00
0.00%
$0.00
$1160.00
Comments: As of January 1st, 2012 ELI will begin charging a $2.00 per sample surcharge for sample management. This fee
will be applied to all solid and aqueous samples.
Quoted prices are based on net 30 days payment of invoices. Discounts will not apply if terms are not met.
Quoted prices reflect standard tum around time of-25 working days. Additional charges may apply for accelerated TAT.
Please advise ELI as to your project specific requirements.
SUBCONTRACT LABORATORY ANALYSIS
Any discounts would not apply for analysis that Is subcontracted to a laboratory outside of an Energy Laboratories, Inc.
facility. Subcontract laboratory prices are subject to change without prior notification.
URANIUM MINE SAMPLES
Any 11e(2) or source material samples are subject to a sample managemenVhandling fee of $50 per work order.
SAMPLE CLEAN UP
Additional charges will apply for any sample with atypical clean up. This will include, but is not limited to additional filters
and/or increased analyst time.
Shipping charges are subject to change based off current UPS prices.
To assure that the quoted analysis and pricing specifications are provided, please include the Quote ID number
referenced above on the Chain of Custody or sample submittal documents.
Page6
Page 172 of 172
[ij =I I Laboratories LLc
a member of The GEL Group INC
PO Box 30712 Cr1a~ eston. SC 29417
2040 Savage Road Cha~ est on. SC 29407
P 843 556.8171
F 843 766.1178
September 17, 2019
Ms. Kathy Weinel
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Re: Tailings 2019 Characterization
WorkOrder:488668
Dear Ms. Weinel:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on August 24, 2019. This revised data report has been prepared and reviewed in
accordance with GEL's standard operating procedures. This package is revised to correct project name.
Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards,
with any exceptions noted. The results reported relate only to the items tested and to the sample as received by
the laboratory. These results may not be reproduced except as full reports without approval by the laboratory.
Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 4289.
Purchase Order: DW16138
Enclosures
Sincerely
Julie Robinson
Project Manager
i111ru1 1111111~1111 111111111111
gel.com
Page 2 of 50 SDG: 488668 Revl
Energy Fuels Resources (USA), Inc.
Tailings 2019 Characterization
SDG: 488668
This package is revised to correct project name.
September 17, 2019
Laboratory Identification:
GEL Laboratories LLC
2040 Savage Road
Charleston, South Carolina 29407
[phone]
Summary:
Receipt Narrative
for
Energy Fuels Resources (USA), Inc.
SDG: 488668
Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on August 24, 2019
for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample
containers arrived without any visible signs of tampering or breakage. There are no additional comments
concerning sample receipt.
Sample Identification: The laboratory received the following samples:
Laboratory ID Cli~nt ID
488668001 Cell I
488668002 Cell 2 Slimes
488668003 Cell 3
488668004 Cell 4A
488668005 Cell 4A LDS
488668006 Cell 4B
488668007 Cell 4B LDS
488668008 Cell 65
Case Narrati e:
Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any
technical or administrative problems during analysis, data review, and reduction are contained in the analytical
case narratives in the enclosed data package.
Page 3 of 50 SDG: 488668 Revl
The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt
Checklist, Data Package Qualifier Definitions and data from the following fractions: General Chemistry and
Radiochemistry.
Page 4 of 50 SDG: 488668 Revl
Julie Robinson
Project Manager
Samples Shipped to:
Project
Annual Tailings 2019
Sample ID
Cell 1
Cell 2Slimes
Cell 3
Cell4A
Cell 4A LDS
Cell48
Cell 48 LDS
Cell65
Sheet 1 of 1
CHAIN OF CUSTODY
Gel Laboratories Contact: Tanner Holliday ------------2040 Savage Road Ph: 435 678 4115
Charleston, SC 29407 [e-mail]
Date
Collected
8/21/2019
8/21/2019
8/21/2019
8/21/2019
8/21/2019
8/21/2019
8/21/2019
8/21/2019
Samplers Name Samplers Signature
Tanner Holliday
Time
Collected
835
905
920
940
945
1015
1030
835
Laboratory Analysis Requested
Dissolved Gross Alpha, Thorium (228, 230, 232) Uranium
(233/234, 235/236, 238), Ra-226, specific gravity
Dissolved Gross Alpha, Thorium (228, 230, 232) Uranium
(233/234, 235/236, 238), Ra-226, specific gravity
Dissolved Gross Alpha, Thorium (228, 230, 232) Uranium
(233/234, 235/236, 238), Ra-226, specific gravity
Dissolved Gross Alpha, Thorium (228, 230, 232) Uranium
(233/234, 235/236, 238), Ra-226, specific gravity
Dissolved Gross Alpha, Thorium (228, 230, 232) Uranium
(233/234, 235/236, 238), Ra-226, specific gravity
Dissolved Gross Alpha, Thorium (228, 230, 232) Uranium
(233/234, 235/236, 238), Ra-226, specific gravity
Dissolved Gross Alpha, Thorium (228, 230, 232) Uranium
(233/234, 235/236, 238), Ra-226, specific gravity
Dissolved Gross Alpha, Thorium (228, 230, 232) Uranium
{233/234, 235/236, 238), Ra-226, specific gravity
Cemments: SAMPLES ARE NOT .Fl~LD FILTERED -PLEA~E FILTER UPON RECEIPT( SAMPLES ARE N0T
PRESERVED -pH-is as collectl;ldl Se_e Julie Robinsan for teetmical questions. No. LOCUS UPLOAD. Methods used :a
same as 432537 ·
Date/Time
Page 5 of 50 SDG: 488668 Revl
,:(, SAMPLE RECEIPT & REVIEW FOR.l.'1
Client: VA/JV/T. SDGIAR/COC/Work Onl•r. . l,19) \-1 (p((l~
CA ~ltl/!ft/ -
Rcccl1•ed Bv: D:itc Rccch·cd:
• I Cit<~bto,
FedEx fa11ress Fcdfa Ground S Field Services Courier O!her
Cariier and Tracking Number _fZ Jq~ YfY t1L f/l's9 3.tl!f~
Suspected ll:u:•nl b1fom1ation ;! .. +ifNcl Counl5 > IOOcpm on samples nol nw!.-cd "mdioac1ivc", oonlact lhc Radiation Safely Group for furtherin\'esli~tion. z:
./ Hazard Class Shipped: UN#:
A)Shiuucd as a DOT Hazardous? lfUN2910, Is lhc Radioactive Shipmen! Survey Complirun? Yes_ No __
I'
Bl Did lhc clienl dcsignalc Ute samples an: 10 be v' COC ootalion or radio.'lclivc slickcis on oonlaincr. equal clien1 designalio11
received as rndioacli,•e?
C) Did tile RSO classify the samples as 'j Maximum Net Counls ~ (Obscivcd Counts -Arca Background Counls): __Q_ O'M I ntR/Hr
radioac1ivc? Clnssiricd as: Rod 1 Rad. 2 Rad J
<./ COC notation or hazaid lnbels on conJaincr. equal client dcsiguntion.
D) Did lltc clield desi!lllale samples are ls-wudous?
./ lfD or Eis yes, select Hazards below .
E) Did lite RSO ideulify J)Ossible hazanls? PCB~ Flanunablc Foreign Soil RCRA Asbestos Beryllium Ober:
Sam11lc Receipt Cri1cria :i < .. Contmcnts/Qualifiers (Required for Non-Confom,ing Items) > z:
Shipping containers received intact nn<l Cin:I: Apµfi<>bl:: Sulsbrokcn D>m;ii:,:d container Lcakin3 aonsoincr Olhcr (describe)
1 !l:aled?
Chain of custody docume1Us irduded Cin:I: Appll<:obl:: Clicl\l contaciod owl pro,idcd COC COC c1ca1cd upon rccs:ip!
2 with shipment?
Samples requiring cold prescrva1ion Prcscrva1iou Mclhod: Wei Jes: Ice P<tcks Dry !cc ~ 01her:
TEMP: C,,/ c::::_ 3 •oll tempcrahues are reconled in Cclsi\LS witlrin (O.< 6 deg, C)?•
Daily check perfomied and passed on JR Tcnipcrntun: Dee ice Serini#: -.L~ ( -,..,
" lcmpernture gun? Sccoudaty Temperature Device Serial # (If Applicnblc):
Cln:le App8:ablo: S"ls brok .. n Dl'ulUli;::cd conUJincr Lc:tl.lns co,unlncr Othor (describe)
5 Sample containers intact and sealed?
Samples requiring chemical preservation S2mpl: ID's ond Con11l11<1$ AJTcclod:
6 al proper pH? If Pn:scn~U•n ruldcd. Loll/:
f!Ycs, an: Encores or Soil Ki1s p1csicnt forsolitls? Yes No NA (l!ycs, lake to VOA Pn:=:r)
Do any samples require Volatile Do liquid VOAvialsco1daiu ocid prcscrvntioo1 Yes No NA (l!unknowu, selccl Nol
7 Analysis·/ J Arc liquid VOA ,•inls free of hc:tdspace'/ Yes_ No_ NA_
Sample ID~ and contliners alfccled:
!D's ond tests nll'ccted:
8 Samples received within holding tinie?
Sample lD's on COC mttcb !D's on ID's and cotdalucrs :i!Tccicd:
9 bottles?
Dale & tim: on COC nnlch dale & time Circle Applicable: No dales on comnincrs No limes on contnincis COC missing info Otltcr (describe)
10 onboltlcs?
Nunbcr of containers received nntch / Circle Applicable: <I!!'_ oulUWIICfCOUIII on ~OUicr(dcscribe)
11 nunber indicated on COCI
12 Are sample containers identifiable as J GEL provided?
COC fonn is properly signed in I Circle Applicable: Not relinquished 011tcr(dcscribc)
13 relinquisliedlrcceivcd sections'?
Co11u11cms (USG Conlinualion Fom1 if nccdcd):
.. ..J> '
··~
• a
PM (or PMAI review: Initials n'--r\ i..:-Date 't\ l..~t>I l"\ Pa~ -l-of_!_ . . .
! GL-CHL-SR-001 Rev6
Page 6 of 50 SDG: 488668 Revl
GEL Laboratories LLC -Login Review Report
GEL Work Order/SDG: 488668
Client SDG: 488668
Annual Tailings 2019
Project Manager:
Project Name:
Purchase Order:
Package Level:
EDD Fonnat:
Julie Robinson
DNMI00107 Tailings 2019 Characterization
DW16138
LEVEL3
EIM_DNMI
Collect
GELID Client Sample ID Client Sample Desc. Date& Time
488668001 Cell 1 21-AUG-19 08:35
488668002 Cell 2 Slimes 21-AUG-19 09:05
488668003 Cell 3 21-AUG-19 09:20
488668004 Cell4A 21-AUG-19 09:40
488668005 Cell4A LOS 21-AUG-19 09:45
488668006 Cell48 21-AUG-19 10:15
488668007 Cell4B LOS 21-AUG-19 10:30
488668008 Cell 65 21-AUG-19 08:35
Product
Client Sample ID Status Tests/Methods Reference
-001 Cell 1 REVW ASTM O 5057 Specific Gravity
REVW Rad 2 Aliquot for distribution
throughout the lab
REVW Alphaspec Th, Liquid
REVW U-233/234,U-235/236 and U-238 U-233/234,U-
235/236
REVW GFPC,Total Alpha Radium, Gross Alpha
Liquid
REVW Lucas Cell, Ra226, liquid
REVW Laboratory Filtration
-002 Cell 2 Slimes REVW ASTM O 5057 Specific Gravity
REVW Rad 2 Aliquot for distribution
throughout the lab
REVW Alphaspec Th, Liquid
REVW u-233/234,U-235/236 and U-238 U-233/234,U-
235/236
REVW GFPC,Total Alpha Radium, Gross Alpha
Liquid
REVW Lucas Cell, Ra226, liquid
REVW Laboratory Filtration
-003 Cell 3 REVW ASTM D 5057 Specific Gravity
REVW Rad 2 Aliquot for distribution
throughout the lab
REVW Alphaspec Th, Liquid
Work Order Due Date: 14-SEP-19
Package Due Date:
EDD Due Date:
Due Date:
EMK
Receive Time # of
Date & Time Zone Cont.
24-AUG-19 09:35 -2 1
24-AUG-19 09:35 -2 1
24-AUG-19 09:35 -2 1
24-AUG-19 09:35 -2 1
24-AUG-19 09:35 -2 1
24-AUG-19 09:35 -2 1
24-AUG-19 09:35 -2 1
24-AUG-19 09:35 -2 1
Fax Date PM Comments
12-SEP-19
14-SEP-19
14-SEP-19
Lab
Matrix
WATER
WATER
WATER
WATER
WATER
WATER
WATER
WATER
Handle these samples carefully,
they are low pH with high
metals. Use container .02 for all
analyse
Handle these samples carefully,
they are low pH with high
metals. Use container .02 for all
analyse
Handle these samples carefully,
they are low pH with high
metals. Use container .02 for all
analyse
Report Date: 17-SEP-19
Work Order: 488668
Page 1 of 5
Collector: C
Prelogin #: 20190895207
Project Workdef ID: 1330584
SDG Status: Closed
Logged by:
Fax Daysto Prelog Lab Field
Due Date Process CofC#
21
21
21
21
21
21
21
21
Aux Data
Group QC QC
Receive
Codes
RAD2
..... > Q) RAD2 e:::
00 \0 \0 00 00 v
C 0 ~
0
\I') RAD2 '+-
C
c--
QJ
OJ (tj
0...
GEL Laboratories LLC -Login Review Report Report Date: 17-SEP-19
Work Order: 488668
Page 2 of 5
REVW u-233/234,U-235/236 and U-238 U-233/234,U-
235/236
REVW GFPC,Total Alpha Radium, Gross Alpha
Liquid
REVW Lucas Cell, Ra226, liquid
REVW Laboratory Filtration
-004 Cell 4A REVW ASTM O 5057 Specific Gravity Handle these samples carefully, RA02
REVW Rad 2 Aliquot for distribution they are low pH with high
metals. Use container .02 for all throughout the lab analyse REVW Alphaspec Th, Liquid
REVW U-233/234,U-235/236 and U-238 U-233/234,U-
235/236
REVW GFPC,Total Alpha Radium, Gross Alpha
Liquid
REVW Lucas Cell, Ra226, liquid
REVW Laboratory Filtration
-005 Cell 4A LOS REVW ASTM O 5057 Specific Gravity Handle these samples carefully, RA02
REVW Rad 2 Aliquot for distribution they are low pH with high
metals. Use container .02 for all throughout the lab analyse REVW Alphaspec Th, Liquid
REVW U-233/234,U-235/236 and U-238 U-233/234,U-
235/236
REVW GFPC, Total Alpha Radium, Gross Alpha
Liquid
REVW Lucas Cell, Ra226, liquid
REVW Laboratory Filtration
-006 Cell 4B REVW ASTM O 5057 Specific Gravity Handle these samples carefully, RA02
REVW Rad 2 Aliquot for distribution they are low pH with high
metals. Use container .02 for all throughout the lab analyse REVW Alphaspec Th, Liquid
REVW U-233/234,U-235/236 and U-238 U-233/234,U-
235/236
REVW GFPC,Total Alpha Radium, Gross Alpha
Liquid
REVW Lucas Cell, Ra226, liquid
REVW Laboratory Filtration --007 Cell 4B LOS REVW ASTM O 5057 Specific Gravity Handle these samples carefully, RA02 t
REVW Rad 2 Aliquot for distribution they are low pH with high i:i::: metals. Use container .02 for all throughout the lab analyse 00
REVW Alphaspec Th, Liquid IC IC
REVW U-233/234,U-235/236 and U-238 U-233/234,U-oe oe 235/236 ~
REVW GFPC,Total Alpha Radium, Gross Alpha c.:; Liquid
REVW Lucas Cell, Ra226, liquid C rr. REVW Laboratory Filtration
-008 Cell 65 REVW ASTM O 5057 Specific Gravity Handle these samples carefully, RA02 C <r.
REVW Rad 2 Aliquot for distribution they are low pH with high <.-metals. Use container .02 for all C throughout the lab analyse oc REVW Alphaspec Th, Liquid Q;
b. c,:
0.-
GEL Laboratories LLC -Login Review Report
REVW U-233/234,U-235/236 and U-238 U-233/234,U-
235/236
REVW GFPC,Total Alpha Radium, Gross Alpha
Liquid
REVW Lucas Cell, Ra226, liquid
REVW Laboratory Filtration
Product: ASP_ THL Workdef ID: 1371096 In Product Group? No
Method: DOE EML HASL-300, Th-01-RC Modified
Product Description: Alphaspec Th, Liquid
Samples: 001,002,003,004,005,006,007, 008
Parmname Check: All parmnames scheduled properly
CAS#
14274-82-9
14269-63-7
7440-29-1
Parmname
Thorium-228
Thorium-230
Thorium-232
Product: ASP _UUL Workdef ID: 1371097 In Product Group? No
Method: DOE EML HASL-300, U-02-RC Modified
Product Description: U-233/234,U-235/236 and U-238
Samples: 001, 002, 003, 004, 005, 006, 007, 008
Parmname Check: All parmnames scheduled properly
CAS# Parmname
13968-55-3/13966-Uranium-233/234
15117-96-1/13982-Uranium-235/236
7440-61-1 Uranium-238
Product: GFCTORAL WorkdeflD: 1371098
Method: EPA 903.0
Product Description: GFPC,Total Alpha Radium, Liquid
Samples: 001,002,003, 004,005,006,007,008
Parmname Check: All parmnames scheduled properly
CAS# Parmname
Gross Radium Alpha
In Product Group? No
Group Name:
Client RDL or
PQL&Unit
Group Name:
Client RDL or
PQL & Unit
Group Name:
Client RDL or
PQL & Unit
Reporting
Units
pCi/L
pCi/L
pCi/L
Report Date: 17-SEP-19
Work Order: 488668
Page 3 of 5
Group Reference:
Path: High Rad
Product Reference:
Moisture Correction: "As Received"
Parm Included Included Custom
Function in Sample? in QC? List?
REG
REG
REG
y
y
y
y
y
y
No
Group Reference:
Path: High Rad
Product Reference: U-233/234,U-235/236
Moisture Correction: "As Received"
Reporting Parm Included Included Custom
Units Function in Sample? in QC? List?
pCi/L
pCi/L
pCi/L
Reporting
Units
pCi/L
REG
REG
REG
y
y
y
y
y
y
No
Group Reference:
Path: High Rad
Product Reference: Gross Alpha
Moisture Correction: "As Received"
Parm Included Included Custom
Function in Sample? in QC? List?
REG y y No
.....
;> ~
00 I.O I.O 00 00 ,e:f"
0 {Z!
0
V)
4-4 0
°' Q)
tl.l ro ~
GEL Laboratories LLC -Login Review Report
Product: LUC26RAL WorkdeflD: 1371099 In Product Group? No
Method: EPA 903.1 Modified
Product Description: Lucas Cell, Ra226, liquid
Samples: 001,002,003,004,005,006,007,008
Parmname Check: All parmnames scheduled properly
CAS# Parmname
13982-63-3 Radium-226
Product: MISSGAS_L WorkdeflD: 1370067 In Product Group? No
Method: ASTM D 5057
Product Description: ASTM D 5057 Specific Gravity
Samples: 001, 002, 003, 004, 005, 006, 007, 008
Parmname Check: All parmnames scheduled properly
CAS# Parmname
Specific Gravity
Product: RADALQT _L WorkdeflD: 1371095 In Product Group? No
Method:
Product Description: Rad 2 Aliquot for distribution throughout the lab
Samples: 001, 002, 003,004,005,006,007, 008
Parmname Check: All parmnames scheduled properly
CAS# Parmname
Product: LABFILT_L Workdef ID: 1473975
Method:
Product Description: Laboratory Filtration
Samples: 001 , 002,003,004,005,006,007,008
Parmname Check: All parmnames scheduled properly
CAS# Parmname
In Product Group? No
Group Name:
Client RDL or
PQL & Unit
1
Group Name:
Client RDL or
PQL & Unit
.1 none
Group Name:
Client RDL or
PQL & Unit
Group Name:
Client RDL or
PQL & Unit
Reporting
Units
pCVL
Reporting
Units
none
Reporting
Units
Reporting
Units
Group Reference:
Report Date: 17-SEP-19
Work Order: 488668
Page 4 of 5
Path: High Rad
Product Reference:
Moisture Correction: "As Received"
Parm Included Included Custom
Function in Sample? in QC? List?
REG y y No
Group Reference:
Path: Standard
Product Reference:
Moisture Correction: "As Received"
Parm Included Included Custom
Function in Sample? in QC? List?
REG y y
Group Reference:
Path: Standard
Product Reference:
No
Moisture Correction: "As Received"
Parm Included Included Custom
Function in Sample? in QC? List?
0
-Group Reference: ~
Path: Standard for High Rad Products Only ~
Product Reference:
Moisture Correction: "As Received"
Parm Included Included Custom
Function in Sample? in QC? List?
0
00 l,O
l,O
00 00 s::t"
6
en
0 V)
4-< 0
0 -(1)
/;)J
cd 11..
GEL Laboratories LLC -Login Review Report
Contingent
Tests
Action
Login Requirements:
Product Name Description
Requirement
Samples
Include? Comments
Peer Review by: ___________ _ Work Order (SDG#), PO# Checked? ____ _
Report Date: 17-SEP-19
Work Order: 488668
Page 5 of 5
C of C signed in receiver location? _____ _
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List of current GEL Certifications as of 17 September 2019
State Certification
Alaska 17-018
Arkansas 88-0651
CUA 4200904046
California 2940
Colorado SC00012
Connecticut PH-0169
DoD ELAP/ISOl7025 A2LA 2567.01
Florida NELAP £87156
Foreign Soils Permit P330-15-00283,P330-15-00253
Georgia SCOOOl2
Georgia SOWA 967
Hawaii SCOOOl2
Idaho SCOOOl2
Illinois NELAP 200029
Indiana C-SC-01
Kansas NELAP E-10332
Kentucky SOWA 90129
Kentucky Wastewater 90129
Louisiana Drinking Water LA024
Louisiana NELAP 03046 (AI33904)
Maine 2019020
Maryland 270
Massachusetts M-SC012
Michigan 9976
Mississippi SC00012
Nebraska NE-OS-26-13
Nevada SC000122020-l
New Hampshire NELAP 2054
New Jersey NELAP SC002
New Mexico SCOOOl2
New York NELAP 11501
North Carolina 233
North Carolina SOWA 45709
North Dakota R-158
Oklahoma 2019-013
Pennsylvania NELAP 68-00485
Puerto Rico SC00012
S. Carolina Radiochem 10120002
South Carolina Chemistry 10120001
Tennessee TN 02934
TexasNELAP Tl04704235-19-l5
UtahNELAP SC000122019-28
Vermont VT87156
Virginia NELAP 460202
Washington C780
Page 12 of 50 SDG: 488668 Revl
Product: Specific Gravity
General Chemistry
Technical Case Narrative
Energy Fuels Resources
SDG #: 488668
Analytical Method: ASTM D 5057
Analytical Procedure: GL-GC-E-065 REV# 7
Analytical Batch: 1913001
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID#
488668001
488668002
488668003
488668004
488668005
488668006
488668007
488668008
Client Sample Identification
Cell I
Cell 2 Slimes
Cell 3
Cell 4A
Cell 4A LDS
Cell 4B
Cell 4B LDS
Cell 65
The samples in this SDG were analyzed on an "as received" basis.
Data Summary:
There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this
report met the acceptance criteria specified in the analytical methods and procedures for initial calibration,
continuing calibration, instrument controls and process controls where applicable.
Certification Statement
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 13 of 50 SDG: 488668 Revl
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Qualifier Definition Report
for
DNMI001 Energy Fuels Resources (USA), Inc.
Client SDG: 488668 GEL Work Order: 488668
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a surrogate compound
ReviewNalidation
GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables
receive a third level review of the fractional data package.
The following data validator verified the information presented in this data report:
Signature:}~ ;11 ~ Name: Kristen Mizzell
Date: 07 SEP 2019 Title: Team Leader
Page 14 of 50 SDG: 488668 Revl
GELLABORATO~ESLLC
2040 Savage Road Charleston, SC 29407 -[phone] -www.gel.com
Contact:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado
Ms. Kathy Weinel
QC Summary
Workorder: 488668
Parmname NOM Sam~le Units RPO%
Notes:
The Qualifiers in this report are defined as follows:
**
<
>
A
B
C
D
E
F
H
M
Analyte is a surrogate compound
Result is less than value reported
Result is greater than value reported
The TIC is a suspected aldol-condensation product
For General Chemistry and Organic analysis the target analyte was detected in the associated blank.
Analyte has been confirmed by GCIMS analysis
Results are reported from a diluted aliquot of the sample
General Chemistry--Concentration of the target analyte exceeds the instrument calibration range
Estimated Value
Analytical holding time was exceeded
Matrix Related Failure
NIA RPD or %Recovery limits do not apply.
NI
ND
NJ
Q
R
u
X
y
z
See case narrative
Analyte concentration is not detected above the detection limit
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
Sample results are rejected
Analyte was analyzed for, but not detected above the CRDL.
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
QC Samples were not spiked with this compound
Paint Filter Test--Particulates passed through the filter, however no free liquids were observed.
Reoort Date: September 17, 2019
REC% Ran e Anlst
/\
d
h
RPD of sample and duplicate evaluated using +I-RL. Concentrations are <SX the RL. Qualifier Not Applicable for Radiochemistry.
5-day BOD--The 2: 1 depletion requirement was not met for this sample
Preparation or preservation holding time was exceeded
Page 1 of
Date Time
NIA indicate that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of4 or more or %RPO not applicable.
/\ The Relative Percent Difference (RPO) obtained from the sample duplicate (DUP) i · evaluated again I. the acceptance criteria when the sample i greater than
five times (SX) the contract required detection limit (RL). In cases where either the sample or duplicate value isles than SX the RL a control limit of +I-the
RL is used to evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
Page 23 of 50 SDG: 488668 Revl
Radiochemistry
Technical Case Narrative
Energy Fuels Resources
SDG #: 488668
Product: Alphaspec Th, Liquid
Analytical Method: DOE EML HASL-300, Th-01-RC Modified
AnaJytical Procedure: GL-RAD-A-038 REV# 18
Analytical Batch: 1914167
Filtration Method: GL-RAD-A-026
Filtration Procedure: GL-RAD-A-026 REV# I 7
Filtration Batch: 1912341
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID#
488668001
488668002
488668003
488668004
488668005
488668006
488668007
488668008
1204374680
1204374681
1204374682
Client Sample Identification
Cell 1
Cell 2 Slimes
Cell 3
Cell 4A
Cell 4A LDS
Cell 4B
Cell 4B LDS
Cell 65
Method Blank (MB)
488668002(Cell 2 Slimes) Sample Duplicate (DUP)
Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
Data Summary:
All sample data provided in this report met the acceptance criteria specified in the analytical methods and
procedures for initial calibration, continuing calibration, instrument controls and process controls where
applicable, with the following exceptions.
Quality Control (QC) Information
RDLMet
The blank (See Below) did not meet the detection limit due to keeping the blank volume consistent with the
other sample aliquots.
Sample Analyte Value
1204374680 (MB) Thorium-228 Result -187 < MDA 729 > RDL 1 pCi/L
Thorium-230 Result 422 < MDA 646 G. RDL 1 pCi/L
Thorium-232 Result 14.2 < MDA 409 > RDL 1 pCi/L
Samples (See Below) did not meet the detection limits due to the small sample aliquots used. The aliquots were
Page 24 of 50 SDG: 488668 Revl
reduced due to the high activity of other isotopes and in attempt to minimize interference.
Sample Analyte Value
1204374681 (Cell 2 SlimesDUP) Thorium-228 Result -2.19 < MDA 222 > RDL 1 pCi/L
Thorium-232 Result 86.5 < MDA 220 > RDL I pCi/L
488668002 (Cell 2 Slimes) Thorium-228 Result 3.58 < MDA 553 > RDL I pCi/L
Thorium-232 Result -36.3 < MDA 378 > RDL I pCi/L
488668003 (Cell 3) Thorium-228 Result 196 < MDA 573 > RDL I pCi/L
Thorium-232 Result 222 < MDA 286 > RDL I pCi/L
Technical Information
Recounts
Sample 1204374680 (MB) was recounted due to a suspected blank false positive. The recount is reported.
Miscellaneou Information
Manual Integration
Manual integration of alpha spectroscopy spectra 488668005 (Cell 4A LDS) was performed to fully separate
counts in Regions of Interest which would have been biased.
Additional Comments
The tracer peak centroid for sample 488668005 (Cell 4A LDS) is greater than 50 keV from the expected library
energy value for the tracer; however, the tracer yield requirement was met and the tracer peak is within the tracer
region of interest.
Product: U-233/234,U-235/236 and U-238
Analytical Method: DOE EML HASL-300, U-02-RC Modified
Analytical Procedure: GL-RAD-A-011 REV# 27
Analytical Batch: 1914171
Filtration Method: GL-RAD-A-026
Filtration Procedure; GL-RAD-A-026 REV# 17
Filtration Batch: 1912341
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID#
488668001
488668002
488668003
488668004
488668005
488668006
488668007
488668008
1204374683
Client Sample Identification
Cell I
Cell 2 Slimes
Cell 3
Cell 4A
Cell 4A LDS
Cell 4B
Cell 4B LDS
Cell 65
Method Blank (MB)
Page 25 of 50 SDG: 488668 Revl
1204374684
1204374685
488668002(Cell 2 Slimes) Sample Duplicate (DUP)
Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
Data .. ummary:
All sample data provided in this report met the acceptance criteria specified in the analytical methods and
procedures for initial calibration, continuing calibration, instrument controls and process controls where
applicable, with the following exceptions.
Quality Control (QC) Information
RDL Met
The blank (See Below) did not meet the detection limit due to keeping the blank volume consistent with the
other sample aliquots.
Sample Analyte Value
1204374683 (MB) Uranium-233/234 Result 147 < MDA 492 > RDL 1 pCi/L
Uranium-235/236 Result 3.22 < MDA 531 > RDL 1 pCi/L
Uranium-238 Result -62.6 < MDA 430 > RDL 1 pCi/L
Sample (See Below) did not meet the detection limit due to the small sample aliquot used. The aliquot was
reduced due to the high activity of other isotopes and in attempt to minimize interference.
Sample Analyte Value
488668003 (Cell 3) Uranium-235/236 Result 109 < MDA 327 > RDL 1 pCi/L
Technical Information
Recounts
Samples 488668003 (Cell 3) and 488668004 (Cell 4A) were recounted due to high MDCs. The recounts are
reported.
Miscellaneous Information
Additional Comments
The tracer peak centroid for sample 1204374683 (MB) is greater than 50 keV from the expected library energy
value for the tracer; however, the tracer yield requirement was met and the tracer peak is within the tracer region
of interest.
Product: GFPC,Total Alpha Radium, Liquid
Analytical Method: EPA 903.0
Analytical Procedure: GL-RAD-A-010 REV# 18
Analytical Batch: 1914172
Page 26 of 50 SDG: 488668 Revl
Filtration Method: GL-RAD-A-026
Filtration Procedure: GL-RAD-A-026 REV# 17
Filtration Batch: 1912341
The following samples were analyzed using the above methods and analytical procedure(s).
Client Sample Identification
Cell l
Cell 2 Slimes
Cell 3
Cell 4A
Cell 4A LDS
Cell 4B
Cell 4B LDS
Cell 65
Method Blank (MB)
GEL Sample ID#
488668001
488668002
488668003
488668004
488668005
488668006
488668007
488668008
1204374686
1204374687
1204374688
1204374689
1204374690
488668003(Cell 3) Sample Duplicate (DUP)
488668003(Cell 3) Matrix Spike (MS)
488668003(Cell 3) Matrix Spike Duplicate (MSD)
Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
Data Summary:
All sample data provided in this report met the acceptance criteria specified in the analytical methods and
procedures for initial calibration, continuing calibration, instrument controls and process controls where
applicable, with the following exceptions.
Quality Control (OC} Information
Duplication Criteria between QC Sample and Duplicate Sample
The Sample and the Duplicate, (See Below), did not meet the relative percent difference requirement; however,
they do meet the relative error ratio requirement with the value listed below.
Sample Analyte Value
1204374687 (Cell 3DUP) Gross Radium Alpha RPD 32.6* (0.00%-20.00%) RER 1.95 (0-3)
RDLMet
The blank (See Below) did not meet the detection limit due to keeping the blank volume consistent with the
other sample aliquots.
Sample Analyte Value
1204374686 (MB) Gross Radium Alpha Result 161 < MDA 189 > RDL 1 pCi/L
Samples 1204374687 (Cell 3DUP), 488668001 (Cell l), 488668002 (Cell 2 Slimes), 488668003 (Cell 3),
488668004 (Cell 4A), 488668005 (Cell 4A LDS), 488668007 (Cell 48 LDS) and 488668008 (Cell 65) did not
meet the client requested detection limit due to limited sample volume.
Technical Information
Recounts
Page 27 of 50 SDG: 488668 Revl
Sample 1204374689 (Cell 3MSD) was recounted due to high recovery. The recount is reported.
Product: Lucas Cell, Ra226, liquid
Analytical Method: EPA 903.1 Modified
Analytical Procedure: GL-RAD-A-008 REV# 15
Analytical Batch: 1914039
Filtration Method: GL-RAD-A-026
Filtration Procedure: GL-RAD-A-026 REV# 17
Filtration Batch: 1912341
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID#
488668001
488668002
488668003
488668004
488668005
488668006
488668007
488668008
1204374364
1204374365
1204374366
1204374367
Client Sample Identification
Cell I
Cell 2 Slimes
Cell 3
Cell 4A
Cell 4A LDS
Cell 4B
Cell 4B LDS
Cell 65
Method Blank (MB)
48866800l(Cell l) Sample Duplicate (DUP)
48866800l(Cell l) Matrix Spike (MS)
Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
Data Summary:
All sample data provided in this report met the acceptance criteria specified in the analytical methods and
procedures for initial calibration, continuing calibration, instrument controls and process controls where
applicable, with the following exceptions.
Quality Control (QC) Information
Duplication Criteria between QC Sample and Duplicate Sample
The Sample and the Duplicate, (See Below), did not meet the relative percent difference requirement; however,
they do meet the relative error ratio requirement with the value listed below.
Sample Analyte Value
1204374365 (Cell lDUP) Radium-226 RPD 45.2* (0.00%-20.00%) RER 2.48 (0-3)
RDLMet
The blank (See Below) did not meet the detection limit due to keeping the blank volume consistent with the
other sample aliquots.
Page 28 of 50 SDG: 488668 Revl
Sample Analyte Value
1204374364 (MB) Radium-226 Result 16.5 < MDA 25.3 > RDL 1 pCi/L
Technica l Information
Recounts
Samples 1204374364 (MB), 1204374367 (LCS) and 488668005 (Cell 4A LDS) were degassed and recounted to
verify sample results. Recounts are reported.
Product: Laboratory Filtration
Filtration Method: GL-RAD-A-026
Filtration Procedure: GL-RAD-A-026 REV# 17
Filtration Batch: 1912341
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID#
488668001
488668002
488668003
488668004
488668005
488668006
488668007
488668008
Client Sample Identification
Cell 1
Cell 2 Slimes
Cell 3
Cell 4A
Cell 4A LDS
Cell 4B
Cell 4B LDS
Cell 65
The samples in this SDG were analyzed on an "as received" basis.
Data Summary:
There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this
report met the acceptance criteria specified in the analytical methods and procedures for initial calibration,
continuing calibration, instrument controls and process controls where applicable.
Certification Statement
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 29 of 50 SDG: 488668 Revl
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 -[phone] -www.gel.com
Qualifier Definition Report
for
DNMI001 Energy Fuels Resources (USA), Inc.
Client SDG: 488668 GEL Work Order: 488668
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a surrogate compound
U Analyte was analyzed for, but not detected above the CRDL.
ReviewNalidation
GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables
receive a third level review of the fractional data package.
The following data validator verified the infonnation presented in this data report:
Signature: j~ ~
Date: 16 SEP 2019
Page 30 of 50 SDG: 488668 Revl
Name: Theresa Austin
Title: Group Leader
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 -[phone] -www.gel.com
QC Summary Reoort Date: September 16, 2019 Energy Fuels Resources (USA), Inc. Page 1 of 225 Union Boulevard
Suite 600
Lakewood, Colorado
Contact: Ms. Kathy Weinel
Workorder: 488668
Parmname NOM SamP-le ual Q_C Units RPO% REC% Rane Anlst Date Time
lligh Rad Testing
3atch 1914039
QC1204374365 488668001 DUP
Radium-226 348 551 pCi/L 45.2* (0%-20%) MXH8 09/12119 11:11
Uncertainty +l-28.0 +l-39.9
QC1204374367 LCS
Radium-226 1350 1180 pCilL 86.9 (75%-125%) 09116119 11 :2,
Uncertainty +l-41.6
QC1204374364 MB
Radium-226 u 16.5 pCilL 09116119 11 :2,
Uncertainty +l-8.23
QC!204374366 488668001 MS
Radium-226 1350 348 1510 pCilL 85.5 (75%-125%) 09112119 11 :0
Uncertainty +l-28.0 +l-64.6
3atch 1914167
QC1204374681 488668002 DUP
Thorium-228 u 3.58 u -2.19 pCi/L NIA NIA JXB7 09111/19 22:Si
Uncertainty +l-128 +l-51.6
Thorium-230 1750 2010 pCilL 13.9 (0%-20%)
Uncertainty +l-362 +l-256
Thorium-232 u -36.3 u 86.5 pCilL NIA NIA
Uncertainty +l-72.3 +l-72.9
QC1204374682 LCS
Thorium-228 19200 pCi/L 09111119 19:2
Uncertainty +I-I 130
Thorium-230 2420 pCilL (75%-125%)
Uncertainty +l-414
Thorium-232 19900 20300 pCi/L 102 (75%-125%)
Uncertainty +l-1160
QC1204374680 MB
Thorium-228 u -187 pCi/L 09112119 13:3
Uncertainty +l-135
Page 47 of 50 SDG: 488668 Revl
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 -[phone] -www.gel.com
QC Summary
Workorder: 488668 Page 2 of
Parmname NOM Sam C Units RPO% REC% Ran e Anlst Date Time
fligh Rad Testing
3atch 1914167
Thorium-230 u 422 pCi/L JXB7 09/12/19 13:3
Uncertainty +/-226
Thorium-232 u 14.2 pCi/L
Uncertainty +/-98.3
3atch 1914171
QC1204374684 488668002 DUP
Uranium-233/234 9300 9990 pCi/L 7.21 (0%-20%) JXB7 09/11/19 19:2
Uncertainty +/-789 +/-876
Uranium-235/236 484 279 pCi/L 53.6 (0%-100%)
Uncertainty +/-214 +/-188
Uranium-238 9150 10400 pCi/L 12.4 (0%-20%)
Uncertainty +/-781 +/-889
QC 12043 74685 LCS
Uranium-233/234 25100 pCi/L 09/11/19 19:2
Uncertainty +/-1350
Uranium-235/236 1990 pCi/L
Uncertainty +/-434
Uranium-238 27300 28600 pCi/L 105 (75%-125%)
Uncertainty +/-1430
QC1204374683 MB
Uranium-233/234 u 147 pCi/L 09/11/19 19:2
Uncertainty +/-149
Uranium-235/236 u 3.22 pCi/L
Uncertainty +/-122
Uranium-238 u -62.6 pCi/L
Uncertainty +/-74.0
3atch 1914172
QC 12043 74687 488668003 DUP
Gross Radium Alpha 3890 5400 pCi/L 32.6* (0%-20%) AXM6 09/12/19 16:5
Uncertainty +/-302 +/-406
QC1204374690 LCS
Gross Radium Alpha l.11E+05 88700 pCi/L 79.9 (75%-125%) 09/12/19 17:1
Uncertainty +/-1400
Page 48 of 50 SDG: 488668 Revl
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 -[phone] -www.gel.com
QC Summar:y
Workorder: 488668
Parmname NOM Sam(lle Qual
fligh Rad Testing
3atch 1914172
QC1204374686 MB
Gross Radium Alpha u
Uncertainty
QC1204374688 488668003 MS
Gross Radium Alpha l.l2E+05 3890
Uncertainty +/-302
QC1204374689 488668003 MSD
Gross Radium Alpha l.l2E+05 3890
Uncertainty +/-302
Notes:
Counting Uncertainty is calculated at the 68% confidence level (]-sigma).
The Qualifiers in this report are defined as follows:
**
<
>
Analyte is a surrogate compound
Result is less than value reported
Result is greater than value reported
The TIC is a suspected aldol-condensation product
QC Units
161 pCi/L
+/-70.3
98100 pCi/L
+/-1540
l.09E+05 pCi/L
+/-1340
RPO%
10.4
A
B
BD
C
D
F
H
K
L
M
M
For General Chemistry and Organic analysis the target analyte was detected in the associated blank.
Results are either below the MDC or tracer recovery is low
Analyte has been confirmed by GC/MS analysis
Results are reported from a diluted aliquot of the sample
Estimated Value
Analytical holding time was exceeded
Analyte present. Reported value may be biased high. Actual value is expected to be lower.
Analyte present. Reported value may be biased low. Actual value is expected to be higher.
M if above MDC and less than LLD
Matrix Related Failure
NIA RPD or %Recovery limits do not apply.
NI See case narrative
ND Analyte concentration is not detected above the detection limit
NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
R Sample results are rejected
U Analyte was analyzed for, but not detected above the CRDL.
UI Gamma Spectroscopy--Uncertain identification
UJ Gamma Spectroscopy--Uncertain identification
Page 49 of 50 SDG: 488668 Revl
REC%
84.l
93.7
Page 3 of
Ran e Anlst Date Time
AXM6 09/12/19 16:5
(75%-125%) 09/12/19 17:l
(0%-20%) 09/13/19 07:2,
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 -[phone] -www.gel.com
QC Summary
Workorder: 488668
Parmname NOM
UL
X
y
A
h
Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
QC Samples were not spiked with this compound
RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
Preparation or preservation holding time was exceeded
Page 4 of
Date Time
NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable.
A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/-the
RL is used to evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
Page 50 of 50 SDG: 488668 Revl
TabD
Chemical and Radiological Summary Tables
Cell 1
Chemical and Radiological Characteristics
Constituent 1987 2003 2007 2008 2009 2010 2011 2012 2013 2013 2014 2015 2016 2017 2018 2018 2019 Resample Resample
Major Ions (mg/L)
Carbonate <5 <l ND ND <1 <1 <l <1 <1 NS <1 <1 <l <l <1 NS <5
Bicarbonate <5 NA ND ND <1 <1 <1 <1 <1 NS <1 <1 <l <l <1 NS <5
Calcium 630 307 483.8 604 635 711 577 426 768 NS 404 573 647 581 518 NS 720
Chloride 8000 6728 37340 9830 20700 7440 33800 78000 9900 NS 11600 25500 19200 19900 39300 NS 19800
Fluoride <100 3005 31.72 0.3 0.4 28.4 69 .2 62.9 4130 NS 2380 5880 2980 4290 5020 NS 3480
Magnesium 7900 5988 21220 6550 16200 5410 14300 16000 4470 NS 5530 12400 9210 9380 20800 NS 9200
Nitrogen-Ammonia 7800 3353 10628 5250 15200 8120 12900 9750 3900 NS 5700 5.4 7090 1040 9810 NS 10400
Nitrogen-Nitrate <100 41.8 269.4 64.9 142 58 212 556 128 NS 53 192 124 152 328 NS 118
Potassium NA 647 5698 1880 4140 1840 4510 9750 6580 NS 3010 7330 1970 2700 4790 NS 2600
Sodium 10000 8638 62600 13200 39000 16700 29500 41700 15900 NS 12200 32100 18900 23900 53500 NS 28000
Sulfate 190000 63667 287600 118000 232000 107000 182000 158000 100000 NS 124000 204000 212000 165000 253000 NS 169000
pH (s.u.) 0.70 1.88 0.80 1.53 1.15 2.73 2.23 1.90 2.74 NS 1.30 1.01 <1.00 <l.00 <l.00 NS 1.14
TDS 120000 94700 357400 131000 140000 130000 216000 342000 149000 NS 159000 334000 242000 231000 361000 NS 257000
Conductivity (umhos/cm) NA NA NA NA 365000 110000 112000 136000 94200 NS 113000 131000 123000 57600 110000 NS 119000
Metals (ug/L)
Arsenic 440000 121267 849000 271000 436000 74400 299000 25500 9800 NS 249000 377000 407000 391000 641000 NS 270000
Beryllium 780 475 2262 500 410 338 1270 3180 415 NS 448 1290 1030 749 1510 NS 930
Cadmium 6600 3990 29320 8790 9120 2940 13700 30700 2380 NS 3060 7710 6320 6730 14000 NS 5400
Chromium 13000 6365 29940 6760 18700 5620 22700 12100 8350 NS 13200 19600 14000 15900 21100 NS 15000
Cobalt 120000 NA 88240 23500 97500 16200 56000 53100 25500 NS 56500 82000 77200 91400 113000 NS 66000
Copper 740000 196667 881000 360000 168000 125000 483000 885000 544000 NS 3420000 3560000 4730000 3440000 4550000 NS 1700000
Iron 3400000 2820000 13480000 3280000 2390000 3400000 8940000 840000 1420000 NS 2520000 6680000 5650000 2300000 12200000 NS 9100000
Lead <20000 3393 27420 11200 10600 9240 23600 17000 2810 NS 13500 16800 22500 23000 41000 NS 22000
Manganese 140000 162500 990200 206000 723000 173000 735000 1560000 188000 NS 162000 515000 713000 510000 936000 NS 540000
Mercury NA NA ND ND 7.61 7.2 61.4 117 6.16 NS 12.5 24.6 8.59 7.86 16.8 NS 3.7
Molybdenum 240000 50550 415600 106000 142000 35300 235000 434000 16800 NS 68800 127000 97100 128000 239000 NS 120000
Nickel 370000 36950 40860 32000 156000 27500 43700 15000 39100 NS 129000 130000 170000 183000 167000 NS 110000
Selenium <20000 1862 15420 13000 14800 5220 11600 8090 2690 NS 3970 7070 3950 5070 10700 NS 10000
Silver <5000 NA 1559.2 449 558 155 1110 4310 329 NS 336 1390 1240 1240 2320 NS 790
Thallium 45000 NA 407.8 165 387 193 560 13 63.3 NS 876 1130 754 155 442 NS <700
Tin <5000 NA 6512 1240 2290 263 1500 <100 <100 NS <17000 <100 <17000 <17000 <17000 NS 540
Uranium 105000 134517 788600 416000 578000 159000 838000 1450000 140000 NS 137000 363000 131000 102000 248000 NS 81000
Vanadium 280000 348000 2208200 1200000 773000 752000 2500000 1940000 98200 NS 485000 1130000 746000 1520000 2440000 NS 1400000
Zinc 1300000 NA 642940 476000 229000 171000 398000 811000 228000 NS 229000 638000 448000 515000 948000 NS 550000
Radiologies (pCi/L)
735000
Gross Alpha NA 1693331 29380 21900 16500 11300 3610 12600 32700 NS 331000 (8/4/2015) 420000 191000 550000 NS 326000 73800
(5/28/2015)
Cell 1
Chemical and Radiological Characteristics
Constituent 1987 2003 2007 2008 2009 2010 2011 2012 2013 2013 2014 2015 2016 2017 2018 2018 2019 Resample Resample
voes (ug/L)
Acetone 35 NA 66.5 110 710 260 80 310 41.1 NS <700 56 40.6 28 50.4 NS 28
Benzene <5 NA ND ND <1 <1 <1 <1 <1 NS <5.0 <1 <1 <l <1 NS <1
Carbon tetrachloride <5 NA ND ND <1 <1 <1 <1 <1 NS <5.0 <1 <1 <l <1 NS <1
Chloroform 8 NA 6.7 6.6 16 4.9 13 19 7.62 NS <70.0 5.54 <1 3.42 114 NS 7.5
Chloromethane NA NA ND 9.4 ll 4.4 3.6 4 5 NS <30.0 1.93 <1 1.13 1.16 NS 2.3
MEK NA NA ND ND 120 65 <l 200 <20 NS <4000 <20 <20 <20 <20 NS 11 J
Methylene Chloride 11 NA ND ND 2 <l <l 2 <1 NS <5.0 1.83 <1 1.09 2.41 NS <1
. Naphthalene <10000 NA <10 ND 1.1 5.4 2 3 <l NS <100 <l <1 <l <1 NS <1
Tetrahydrofuran NA NA 150 <20 <100 <10 <500 2.9 <l NS <46.0 <l <1 <l 4.93 NS <35
Toluene <5 NA ND ND <l <1 <l <1 <l NS <1000 <l <1 <l <1 NS <1
Xylenes <5 NA ND ND <1 <l <l <1 <l NS <10000 <l <l <l <1 NS <l
SVOCS (ug/L)
1,2,4-Trichlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
1,2-Dichlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
1,3-Dichlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
1,4-Dichlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
1-Methylnaphthalene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
2,4,5-Trichlorophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
2,4,6-Trichlorophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
2,4-Dichlorophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
2,4-Dimethylphenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
2,4-Dinitrophenol NA NA NA NA <250 <20 <20 <20 <21.6 <20 <20 <20 <10 <10 <148 <8.04 <50
2,4-Dinitrotoluene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
2,6-Dinitrotoluene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
2-Chloronaphthalene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
2-Chlorophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
2-Methylnaphthalene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8 .04 <10
2-Methylphenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
2-Nitrophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
3&4-Methylphenol NA NA NA NA <22 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
3,3-Dichlorobenzidine NA NA NA NA <100 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <50
4,6-Dinitro-2-NA NA NA NA <250 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <50 methyl phenol
4-Bromophenyl phenyl NA NA NA NA <50 <10 <10 <10 ether <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
4-Chloro-3-methylphenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
4-Chlorophenyl phenyl NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10 ether
4-Nitrophenol NA NA NA NA <250 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8 .04 <50
Acenaphthene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8 .04 <10
Acenaphthylene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8 .04 <10
Anthracene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8 .04 <10
Azobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Benz(a)anthracene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Cell 1
Chemical and Radiologic.al Characteristics
Constituent 1987 2003 2007 2008 2009 2010 2011 2012 2013 2013 2014 2015 2016 2017 2018 2018 2019 Resample Resample
Benzidine NA NA NA NA <100 <10 <10 <10 <10.8 <10 41 <10 <10 <10 <148 <8.04 <100
Benzo(a)pyrene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Benzo(b )fluoranthene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Benzo(g,h,i)perylene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Benzo(k)fluoranthene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Bis(2-chloroethoxy) NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10 methane
Bis(2-chloroethyl) ether NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
B is(2-chloroisopropyl) NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10 ether
B is(2-ethylhexyl) NA NA NA NA <50 27 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10 phthalate
Butyl benzyl phthalate NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Chrysene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Dibenz( a,h )anthracene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Diethyl phthalate NA NA NA NA 170 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Dimethyl phthalate NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Di-n-butyl phthalate NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Di-n-octyl phthalate NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Fluoranthene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Fluorene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
I-Iexachlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
I-Iexachlorobutadiene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <30
I-Iexachloro -NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10 cyclopentadiene
I-Iexachloroethane NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <30
Indeno(l ,2,3-cd)pyrene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Isophorone NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Naphthalene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Nitrobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
N-Nitrosodimethylamine NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
N-Nitrosodi-n-NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10 propylamine
N-Nitrosodiphenylamine NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Pentachlorophenol NA NA NA NA <250 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <50
Phenanthrene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Phenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Pyrene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <10
Pyridine NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 <10 <10 <10 <148 <8.04 <20
1 I-Iistoric values reported for Gross Alpha from 1987 and 2003 are total gross alpha reported in pCi/L. All other gross alpha data are reported as Gross Alpha minus Rn & U.
CeJI 2 Slimes Drain
Chemical and Radiological Characteristics
Constituents 2007 2008 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019
Major Ions (mg/L)
Carbonate ND ND <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <5
Bicarbonate ND ND <1 <1 <1 <1 <1 <1 <1 <1 <l <1 <5
Calcium 572 528 508 496 474 462 465 322 524 402 477 538 480
Chloride 3700 3860 2750 3510 3110 3730 3270 3720 3850 4040 3820 4310 3870
Fluoride 3.3 ND <0.1 2.4 2.1 1.32 161 130 204 48.4 110 116 105
Magnesium 4100 4030 3750 3790 3640 3760 3320 2780 3810 3570 3630 4470 3700
Nitrogen-Ammonia 4020 3620 3240 3820 2940 3540 1880 3500 367 3800 500 5620 4420
Nitrogen-Nitrate 30.9 20.3 38 126 38 27 47.2 35 1.06 12.7 13.7 12.1 33.0
Potassium 636 560 689 620 636 611 622 489 659 512 668 774 710
Sodium 4050 4600 4410 4770 4590 4380 3980 3130 4800 4690 4810 5290 4600
Sulfate 60600 74000 72200 63700 64200 58300 83700 62200 57800 83900 58300 63300 67000
pH (s.u.) 3.18 3.24 3.11 3.39 3.18 3 3.02 3.1 3.1 2.99 3.08 2.89 3.07
TDS 84300 74600 84100 79900 80200 83800 92200 87000 88200 93100 85900 99900 94300
Conductivity (umhos/cm) NA NA 88700 60200 51400 52900 51100 54100 58800 44500 52600 58200 55700
Metals (ug/L)
Arsenic 26900 19300 14200 23500 17800 19400 21000 19800 13300 16900 21100 19600 23000
Beryllium 298 245 271 267 231 251 262 197 275 259 261 241 280
Cadmium 5500 5840 5510 6370 5580 5290 5780 6480 6260 6610 6790 6380 6500
Chromium 2750 2450 2230 2510 2380 2350 2290 1630 1840 1630 2290 2100 2100
Cobalt 46500 43800 38700 48200 42500 48700 44900 46700 46000 46100 50600 46900 54000
Copper 106000 154000 170000 148000 132000 138000 137000 126000 143000 156000 148000 136000 160000
Iron 2770000 3310000 3230000 2720000 2960000 2850000 2810000 2180000 3000000 3410000 3430000 3030000 3600000
Lead 566 528 403 586 501 619 515 638 268 484 593 589 590
Manganese 117000 130000 160000 144000 123000 141000 122000 98000 136000 149000 151000 137000 170000
Mercury ND ND <0.5 <4 11.1 1.9 <0.5 <0.0020 <0.5 <2.00 <2.00 <2.00 <0.2
Molybdenum 4080 3190 2240 4630 3510 3610 3650 4250 2010 3360 4060 3340 3200
Nickel 123000 122000 108000 126000 111000 125000 108000 127000 120000 134000 133000 121000 140000
Selenium 422 647 726 844 714 711 678 1020 631 615 683 635 1300
Silver ND ND <10 <10 <10 <10 <10 <100 <20 <100 <100 <100 <50
Thallium 361 703 368 470 371 338 278 402 233 212 373 374 390
Tin ND ND <100 <100 <100 <100 <100 <17000 <100 <17000 <17000 <17000 <50
Uranium 23000 29200 29900 30600 27100 33400 22800 26400 27200 27300 28600 25200 29000
Vanadium 409000 463000 536000 469000 454000 475000 452000 497000 513000 497000 534000 516000 500000
Zinc 767000 750000 582000 652000 574000 639000 631000 405000 702000 764000 760000 728000 850000
Radiologies (pCi/L)
Gross Alpha 1290 1570 1580 1000 1230 1370 2270 6890 7210 5660 4570 7520 3790 (2400)* -voes (ug/L)
Acetone 550 410 570 460 690 600 384 <700 599 473 551 551 449
Benzene ND ND <1 <1 <l <1 <1 <5.0 <1 <1 <l <1 <1
Carbon tetrachloride ND ND <1 <1 <1 <1 <1 <5.0 <1 <l <1 <1 <1
Chloroform 20 17 16 15 20 16 21.4 <70.0 18.6 15 17.1 17.1 16
Chloromethane 1.8 ND 2.2 2.3 2 3 2.04 <30.0 <1 <1 1.46 1.46 2.2
Cell 2 Slimes Drain
Chemical and Radiological Characteristics
Constituents 2007 2008 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019
MEK 65 ND 100 83 130 100 95.5 <4000 102 80.3 58.4 58.4 135
Methylene Chloride ND ND <1 <1 <l <1 <l <5.0 <l <l 1.02 1.02 0.49 J
Naphthalene 14 7.5 16 17 13 12 16.8 <100 16.2 11.9 10.1 10.1 13
Tetrahydrofuran 15 NA <100 <10 <10 3.2 3.98 <46.0 2.16 <l 2.88 2.88 <10
Toluene 1.7 ND 2.6 2.6 3 2 3.23 <1000 3.74 2.94 3.20 3.20 2.4
Xylenes 1.5 ND <l 2.2 <l 2 5.97 <10000 <1 <l <l <l 0.51 J
SVOCS (ug/L)
l ,2,4-Trichlorobenzene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
1,2-Dichlorobenzene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
1,3-Dichlorobenzene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
1,4-Dichlorobenzene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
1-Methylnaphthalene NA NA <11 <10 <10 <10 <10 11 <10 <10 <10 <9.03 12
2,4,5-Trichlorophenol NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
2,4,6-Trichlorophenol NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
2,4-Dichlorophenol NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
2,4-Dimethylphenol NA NA <51 <20 <20 <10 <10 <10 <10 <10 <10 <9.03 <10
2,4-Dinitrophenol NA NA <1 l <10 <10 <20 <20 <20 <20 <10 <10 <9.03 <50
2,4-Dinitrotoluene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
2,6-Dinitrotoluene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
2-Chloronaphthalene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
2-Chlorophenol NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
2-Methylnaphthalene NA NA <11 <10 <10 <10 <10 11 <10 11.1 <10 <9.03 11
2-Methylphenol NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
2-Nitrophenol NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
3&4-Methylphenol NA NA <21 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
3,3, -Dichlorobenzidine NA NA <51 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <46
4,6-Dinitro-2-methylphenol NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <50
4-Bromophenyl phenyl ether NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
4-Chloro-3-methylphenol NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
4-Chlorophenyl phenyl ether NA NA <51 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
4-Nitrophenol NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <50
Acenaphthene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Acenaphthylene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Anthracene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Azobenzene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Benz(a)anthracene NA NA <21 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Benzidine NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <92
Benzo(a)pyrene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Benzo(b )fluoranthene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Benzo(g,h,i )pery Jene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Benzo(k)fluoranthene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Bis(2-chloroethoxy )methane NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Bis(2-chloroethyl) ether NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Bis(2-chloroisopropyl) ether NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Cell 2 Slimes Drain
Chemical and Radiological Characteristics
Constituents 2007 2008 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019
Bis(2-ethylhexyl) phthalate NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 1.1
Butyl benzyl phthalate NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Chrysene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Dibenz( a,h)anthracene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Diethyl phthalate NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Dimethyl phthalate NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 1.5
Di-n-butyl phthalate NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Di-n-octyl phthalate NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Fluoranthene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Fluorene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Hexachlorobenzene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Hexachlorobutadiene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <28
Hexachlorocyclopentadiene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Hexachloroethane NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <28
Indeno( 1,2,3-cd)pyrene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Isophorone NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Naphthalene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 5.3
Nitro benzene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
N-Nitrosodimethylamine NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
N-Nitrosodi-n-propylamine NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
N-Nitrosodiphenylamine NA NA <51 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Pentachlorophenol NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <50
Phenanthrene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Phenol NA NA <11 10.7 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Pyrene NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <10
Pyridine NA NA <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.03 <18
* Sample was reanalyzed due to comparability with the duplicate sample. The reanalysis data are in (parenthesis).
Cell2LDS
Chemical and Radiological Characteristics
Constituent 2009 2010 2011 2Ql'2 2013 ~.2014 I 20Ts i i 2016 2017 2Qf8 2019
-Major Ions ,lmglli)
Carbonate <1 <1
Bicarbonate 168 324
Calcium 711 615
Chloride 1750 1360
Fluoride 0.4 0.4
Magnesium 596 454
Nitrogen-Ammonia 32.6 0.7 Not Not Not Not Not Not Not Not Not
Nitrogen-Nitrate 2.8 2.2 Sampled Sampled Sampled Sampled Sampled Sampled Sampled Sampled Sampled
Potassium 22 13
Sodium 412 318
Sulfate 2700 1780
pH (s.u.) 6.6 7.36
TDS 6750 5310
Conductivity (umhos/cm) 11000 6500
Meta.ls (ug/L)
Arsenic <5 <5
Beryllium <0.50 <0.50
Cadmium 33.4 1.1
Chromium <25 <25
Cobalt 314 <10
Copper 59 12
Iron 208 37
Lead <1.0 <1.0
Manganese 1810 395 Not Not Not Not Not Not Not Not Not Mercury <0.50 0.52
Molybdenum 21 13 Sampled Sampled Sampled Sampled Sampled Sampled Sampled Sampled Sampled
Nickel 948 <20
Selenium 7.9 9.4
Silver <10 <10
Thallium 0.92 <0.50
Tin <100 <100
Uranium 83.8 79.6
Vanadium 22 <15
Zinc 4220 78
Cell2 LDS
Chemical and Radiological Characteristics
Constituent 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019
Radiologies '(pCi/L)
Gross Alpha 13.5 7.3 Not Not Not Not Not Not Not Not Not
Sampled Sampled Sampled Sampled Sampled Sampled Sampled Sampled Sampled
voes (ug/L)
Acetone <20 <20
Benzene <1 <1
Carbon tetrachloride <1 <1
Chlorofonn <1 <1
Chloromethane <1 <1 Not Not Not Not Not Not Not Not Not MEK <20 <20 Sampled Sampled Sampled Sampled Sampled Sampled Sampled Sampled Sampled Methylene Chloride <1 <1
Naphthalene <1 <1
Tetrahydrofuran <100 6.13
Toluene <1 <1
Xylenes <1 <I
SVOCS (ug/L)
1,2,4-Trichlorobenzene NA <10
1,2-Dichlorobenzene NA <10
1,3-Dichlorobenzene NA <10
1,4-Dichlorobenzene NA <10
1-Methylnaphthalene NA <10
2,4,5-Trichlorophenol NA <10
2,4,6-Trichlorophenol NA <10
2,4-Dichlorophenol NA <10
2,4-Dimethylphenol NA <10
2,4-Dinitrophenol NA <20 Not Not Not Not Not Not Not Not Not 2,4-Dinitrotoluene NA <10 Sampled Sampled Sampled Sampled Sampled Sampled Sampled Sampled Sampled
2,6-Dinitrotoluene NA <10
2-Chloronaphthalene NA <10
2-Chlorophenol NA <10
2-Methylnaphthalene NA <10
2-Methylphenol NA <10
2-Nitrophenol NA <10
3&4-Methylphenol NA <10
3,3 '-Dichlorobenzidine NA <10
4,6-Dinitro-2-methylphenol NA <10
4-Bromophenyl phenyl ether NA <10
Cell 2 LDS
Chemical and Radiological Characteristics
Constituent 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019
4-Chloro-3-methylphenol NA <10
4-Chlorophenyl phenyl ether NA <10
4-Nitrophenol NA <10
Acenaphthene NA <10
Acenaphthylene NA <10
Anthracene NA <10
Azobenzene NA <10
Benz(a)anthracene NA <10
Benzidine NA <10
Benzo(a)pyrene NA <10
Benzo(b )fluoranthene NA <10
Benzo(g,h,i)perylene NA <10
Benzo(k)fluoranthene NA <10
Bis(2-chloroethoxy )methane NA <10
Bis(2-chloroethyl) ether NA <10
Bis(2-chloroisopropyl) ether NA <10
Bis(2-ethylhexyl) phthalate NA <10
Butyl benzyl phthalate NA <10
Chrysene NA <10
Dibenz( a,h )anthracene NA <10
Diethyl phthalate NA <10 Not Not Not Not Not Not Not Not Not
Dimethyl phthalate NA <10 Sampled Sampled Sampled Sampled Sampled Sampled Sampled Sampled Sampled
Di-n-butyl phthalate NA <10
Di-n-octyl phthalate NA <10
Fluoranthene NA <10
Fluorene NA <10
Hexachlorobenzene NA <10
Hexachlorobutadiene NA <10
Hexachlorocyclopentadiene NA <10
Hexachloroethane NA <10
Indeno( 1,2,3-cd)pyrene NA <10
Isophorone NA <10
Naphthalene NA <10
Nitro benzene NA <10
N-Nitrosodimethylamine NA <10
N-Nitrosodi-n-propylamine NA <10
N-Nitrosodiphenylamine NA <10
Pentachlorophenol NA <10
Phenanthrene NA <10
Phenol NA <10
Pyrene NA <10
Pyridine NA <10
Cell 3
em1ca an 10 021ca Ch . I d Rad. I . J Ch aracteristlcs
2013 2018 2019 Constituent 1987 2003 (Avg) 2007 (Avg) 2008 2009 2010 2011 2012 2013 ReSample 2014 2015 2016 2017 2018 ReSample
Major Ions (mg/L)
-Carbonate NA <1 ND ND <1 <1 <1 <1 <1 NS <1 <1 <1.00 <1.00 <l.00 NS <5
Bicarbonate <5 NA ND ND <1 <1 <1 <1 <1 NS <1 <l <l.00 <1.00 <1.00 NS <5
Calcium 300 418 887 478 628 560 200 591 586 NS 294 713 148 526 498 NS 510
Chloride NA 2460 15965 15400 17200 3470 40400 8880 38400 NS 7200 22800 115000 2720 55200 NS 15000
Fluoride <100 667 42.8 1.4 0.6 54.8 64.1 2300 12400 NS 1330 5410 46500 189 7400 NS 1340
Magnesium 5400 3386 15767 13100 17100 2500 22100 5680 15400 NS 1910 12700 31000 84400 22000 NS 10000
Nitrogen-Ammonia 13900 1302 13867 9010 21600 2650 6470 6840 100 NS 3030 8.91 6270 88.5 9490 NS 9000
Nitrogen-Nitrate <100 20 102 44 142 26 261 64 277 NS 59.5 26 .6 582 107 710 NS 925
Potassium NA 254 6657 4760 3820 782 2590 1190 2110 NS 386 1620 3120 133 1480 NS 630
Sodium 5900 3198 25583 22900 28600 5620 47900 6660 34400 NS 3630 23800 59800 2120 46900 NS 14000
Sulfate 180000 33400 173667 167000 214000 40400 197000 80000 440000 NS 37000 158000 834000 9970 208000 NS 96000
pH (s.u.) 0.82 2.28 1.6 1.79 1.4 2.18 1.27 2.4 1.05 NS 2.2 1.72 <1.00 3.63 1.32 NS 3.88
TDS 189000 51633 228500 193000 243000 56200 296000 120000 410000 NS 70100 238000 887000 17300 327000 NS 143000
Conductivity (umhos/cm) NA NA NA NA 304000 59800 86400 80300 84300 NS 56200 121000 13600 20300 104000 NS 95500
Metals (ug/L)
Arsenic 163000 32867 256500 489000 ND 52900 263000 4340 66000 NS 2920 21500 194000 870 20900 NS 380
Beryllium 540 430 913 840 905 206 1570 678 2570 NS 222 1520 12500 590 2950 NS 350
Cadmium 2600 1958 9260 15400 ND 1960 12200 3460 24000 NS 2550 14800 41000 1190 52100 NS 7400
Chromium 12000 3742 14883 12800 ND 3360 22800 10900 30600 NS 2380 15300 76200 <100 25100 NS 230J
Cobalt 48000 NA 82783 57000 ND 13000 76000 76100 99700 NS 20800 72500 74200 4440 120000 NS 64000
Copper 360000 87333 505000 345000 ND 89000 768000 379000 954000 NS 139000 511000 3000000 9720 515000 NS 35000
Iron 2100000 1278333 4874500 4400000 5970000 1460000 10200000 3400000 9700000 NS 688000 4570000 15400000 262000 13300000 NS 2500000
Lead <20000 2507 9647 16900 ND 17200 16700 1860 14400 NS 1900 9090 4030 15.8 20500 NS <75
Manganese 82000 144000 496833 313000 ND 101000 587000 3110000 2470000 NS 214000 1270000 5690000 102000 4070000 NS 1000000
Mercury ND NA ND 16 ND <4 30.9 9.6 21.6 NS 2.4 7.01 873 <2 .00 430 NS 0.20
Molybdenum 52000 12250 122167 209000 14 21300 96200 790 56100 NS 2930 12500 133000 70.1 3740 NS 550
Nickel 170000 20917 131833 241000 ND 23800 75800 150000 122000 NS 44900 121000 29200 7220 113000 NS 150000
Selenium <2000 910 5856 10200 ND 3080 6900 2460 7060 NS 1370 4330 3170 306 3680 NS 2900
Silver <2500 NA 305 1010 ND 101 792 1850 3380 NS 329 1790 6780 <100 3770 NS 110
Thallium 4700 NA 446 1200 ND 190 518 1080 694 NS 290 602 2160 21.3 3760 NS 170
Tin NA NA 1090 1070 ND 155 325 <100 <100 NS <17000 <100 <17000 <17000 <17000 NS <50
Uranium 118000 67833 332333 636000 3690 180000 458000 835000 1200000 NS 134000 530000 5360000 9630 1110000 NS 19000
Vanadium 210000 158333 935000 1130000 ND 692000 2370000 836000 3220000 NS 454000 1720000 10300000 5600 2420000 NS 54000
Zinc 590000 NA 748833 515000 ND 134000 726000 652000 1430000 NS 155000 899000 7810000 68100 2100000 NS 950000
Cell 3
em1ca an .10 Ol!IC Ch . l d Rad" l . a1 Ch aracter1sbcs
2013 11 2018 2019 Constituent 1987 2003 (Avg) 2007 (Avg) 2008 2009 2010 2011 2012 2013 ReSample 2014 2015 2016 2017 2018 ReSample
-Radiologies (pCi/L)
94900
Gross Alpha NA 1015831 16533 21700 17000 4030 11100 1530 81900 NS 19700 (8/4/2015) 86000 292 19700 NS 3890 8780
(5/28/2015)
voes (ug/L)
Acetone 28 NA 80 100 67 37 330 64 302 159 <700 82.8 <200 48.4 135 NS 135
Benzene <5 NA ND ND <1 <1 <1 <1 <5 <1 <5.0 <1 <1 <1 <1 NS <1
Carbon tetrachloride <5 NA ND ND <1 <1 <1 <1 <5 <1 <5.0 <1 <1 <1 <1 NS <1
Chloroform 6 NA ND 11 4.2 2.6 31 2 56.3 21 <70.0 1.75 13.2 <1 5.02 NS 18
Chloromethane NA NA ND ND 1.4 1.8 3.5 1 <5 2.58 <30.0 1.03 19.8 <1 5.36 NS 2.8
MEK NA NA ND ND <1 <1 67 <20 <100 24.5 <4000 <20 <20 <20 <20 NS 34
Methylene Chloride 10 NA ND ND <1 <1 7.4 <1 6.95 <1 <5.0 <1 <1 <1 10.4 NS 0.67 J
Naphthalene <10000 NA ND <10 <1 2.1 1.2 <1 <5 <1 <100 <1 <1 <1 <1 NS 0.57 J
Tetrahydrofuran NA NA 150 <20 <100 <10 <10 <1 <5 <1 <46.0 <1 <1 <1 3.01 NS <35.0
Toluene <5 NA ND ND <1 <1 <1 <1 <5 <1 <1000 <1 <1 <1 <1 NS <1
Xylenes <5 NA ND ND <1 <1 <1 <1 <5 <1 <10000 <1 <1 <1 <1 NS <1
SVOCS (ug/L)
1,2,4-Trichlorobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
1,2-Dichlorobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
1,3-Dichlorobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
1,4-Dichlorobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
1-Methylnaphthalene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
2,4,5-Trichlorophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
2,4,6-Trichlorophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
2,4-Dichlorophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
2,4-Dimethylphenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
2,4-Dinitrophenol NA NA NA NA <53 <20 <20 <20 <21.1 <20 <20 <20 <10 <10 <1,490 <7.78 <50
2,4-Dinitrotoluene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
2,6-Dinitrotoluene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
2-Chloronaphthalene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
2-Chlorophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
2-Methylnaphthalene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
2-Methylphenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
2-Nitrophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
3&4-Methylphenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
3,3, -Dichlorobenzidine NA NA NA NA <21 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <45
4,6-Dinitro-2-methylphenol NA NA NA NA <53 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <50
4-Bromophenyl phenyl ether NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
4-Chloro-3-methylphenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
4-Chlorophenyl phenyl ether NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
4-Nitrophenol NA NA NA NA <53 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <50
Acenaphthene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Cell 3
em1ca an a 10 Ol!lca Ch . I d R d" I . J Ch aractensbcs
2013 2018 2019 Constituent 1987 2003 (Avg) 2007 (Avg) 2008 2009 2010 2011 2012 2013 ReSample 2014 2015 2016 2017 2018 ReSample
Acenaphthylene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Anthracene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Azobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Benz(a)anthracene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Benzidine NA NA NA NA <21 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <l,490 <7.78 <10
Benzo(a)pyrene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Benzo(b )fluoranthene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Benzo(g,h,i)perylene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Benzo(k)fluoranthene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
B is(2-chl oroethoxy )methane NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Bis(2-chloroethyl) ether NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Bis(2-chloroisopropyl) ether NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Bis(2-ethylhexyl) phthalate NA NA NA NA <11 10.6 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Butyl benzyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Chrysene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Di benz( a, h )anthracene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Diethyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1 ,490 <7.78 <10
Dimethyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Di-n-butyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Di-n-octyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Fluoranthene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Fluorene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Hexachlorobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Hexachlorobutadiene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <l,490 <7.78 <27
Hexachlorocyclopentadiene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1 ,490 <7.78 <10
Hexachloroethane NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <27
Indeno( 1,2,3-cd)pyrene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Isophorone NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Naphthalene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Nitrobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
N-Nitrosodimethy I amine NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
N-Nitrosodi-n-propylamine NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
N-Nitrosodiphenylamine NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Pentachlorophenol NA NA NA NA <53 <10 <IO <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <50
Phenanthrene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Phenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Pyrene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <10
Pyridine NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10 <10 <10 <10 <1,490 <7.78 <18
1 Historic values reported for Gross Alpha from 1987 and 2003 are total gross alpha reported in pCi/L. All other gross alpha data are reported as Gross Alpha minus Rn & U.
Cell 4A
Chemical and Radiological Characteristics
Constituent 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019
Major Ions (mg/L)
Carbonate <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <5
Bicarbonate <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <5
Calcium 627 598 558 591 668 445 604 632 607 707 510
Chloride 4650 7350 5870 4980 4530 5900 6410 7040 8060 10100 8670
Fluoride 0.3 21.6 30.6 43 1130 1290 1660 2030 1420 2000 1650
Magnesium 3250 4940 4720 2230 3660 2990 3910 3550 4360 7030 4100
Nitrogen-Ammonia 3140 5230 4930 1540 1340 2730 11 4770 924 9060 6700
Nitrogen-Nitrate 28 52 44 27 38.2 39.5 19.9 41.9 53.4 73.4 70.4
Potassium 980 1440 1450 558 773 724 1020 915 1500 2020 1200
Sodium 5980 11300 11400 7130 6860 7190 9760 9580 12000 17600 15000
Sulfate 67600 87100 267000 64900 83300 64900 77200 126000 77800 116000 81300
pH (s.u.) 1.4 1.99 1.73 1.2 1.47 1.7 1.51 1.59 1.53 1.25 2.40
TDS 81400 107000 108000 76000 90000 97000 104000 124000 120000 147000 122000
Conductivity (umhos/cm) 131000 101000 82100 78100 66300 73000 89600 81300 89800 115000 81400
Metals (ug/L)
Arsenic 626000 109000 86600 60500 73700 70000 82600 94400 104000 125000 63000
Beryllium 296 215 323 167 247 190 281 320 440 538 420
Cadmium 1920 3670 2190 844 1450 1780 2090 2850 3360 3850 2500
Chromium 3220 7500 5900 5990 5220 4620 5460 7920 8520 9350 7200
Cobalt 9440 26500 22500 22900 22900 27500 26100 32800 37900 41000 28000
Copper 99200 168000 181000 433000 540000 556000 477000 566000 578000 683000 580000
Iron 2360000 2920000 3390000 3190000 2620000 2280000 3090000 3850000 4480000 5320000 3200000
Lead 5360 11800 11000 5270 11500 14800 11700 14000 15100 16400 9000
Manganese 178000 209000 131000 112000 143000 120000 181000 225000 261000 307000 210000
Mercury 1.19 <4 15.2 2.4 0.786 2.5 0.99 <2 2.30 2.52 2.1
Molybdenum 24300 43800 24200 58200 25500 40600 35400 43900 40800 59100 19000
Nickel 17100 40900 43500 41300 43300 54100 48700 61300 66800 71900 50000
Selenium 4620 5810 4460 1310 2080 2000 2400 2820 4450 5870 3700
Silver 78 193 216 127 144 197 186 305 379 521 310
Thallium 162 350 410 250 256 376 436 568 169 727 90
Tin 257 378 319 169 118 <17000 142 <17000 <17000 <17000 77
Uranium 118000 217000 153000 91000 112000 159000 171000 214000 193000 244000 35000
Vanadium 918000 1090000 730000 237000 461000 535000 577000 715000 972000 1080000 150000
Zinc 142000 224000 286000 200000 183000 169000 237000 318000 344000 406000 280000
Cell 4A
Chemical and Radiological Characteristics
Constituent 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019
Radiologies (pCi/.L)
176000
Gross Alpha 8910 3400 8290 16300 15800 240000 (8/4/2015) 292000 133000 516000 261000 37800
(5/28/2015)
voes (ug/L)
Acetone 60 55 100 25 28.4 <700 42.5 45.1 21.4 42.7 39 J
Benzene <l <1 <1 <1 <l <5.0 <1 <l <l <1 <2.5
Carbon tetrachloride <l <l <1 <l <1 <5.0 <1 <1 <l <1 <2.5
Chloroform 4 8.5 10 <l <1 <70.0 <l <l <1 1.91 1.9 J
Chloromethane 3.4 5.5 7.9 <1 <1 <30.0 <1 <l 1.35 1.76 1.7 J
MEK <l <1 <l <1 <20 <4000 <20 <20 <20 <20 13 J
Methylene Chloride <1 <1 <1 <20 <1 <5.0 <1 <1 <l <l <2.5
Naphthalene 1.8 <1 <1 <1 <1 <100 <1 <l <1 <1 <2.5
Tetrahydrofuran <100 <10 <10 1.36 <1 <46.0 <l 12.6 <1 <l <35.0
Toluene <l <1 <1 <l <1 <1000 <l <1 <l <l <2.5
Xylenes <l <l <l <l <l <10000 <1 <1 <l <l <2.5
SVOCS (ug/L)
1,2,4-Trichlorobenzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
1,2-Dichlorobenzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
1,3-Dichlorobenzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
1,4-Dichlorobenzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
1-Methy !naphthalene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
2,4,5-Trichlorophenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
2,4,6-Trichlorophenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
2,4-Dichlorophenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
2,4-Dimethylphenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
2,4-Dinitrophenol <53 <20 <20 <20 <20 <20 <20 <10 <10 <8.57 <50
2,4-Dinitrotoluene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
2,6-Dinitrotoluene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
2-Chloronaphthalene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
2-Chlorophenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
2-Methylnaphthalene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
2-Methylphenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
2-Nitrophenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
3&4-Methylphenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
3,3, -Dichlorobenzidine <21 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <46
4,6-Dinitro-2-methylphenol <53 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <50
4-Bromophenyl phenyl ether <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
4-Chloro-3-methylphenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
4-Chlorophenyl phenyl ether <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
4-Nitrophenol <53 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <50
Acenaphthene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Acenaphthylene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Cell 4A
Chemical and Radiological Characteristics
Constituent 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019
Anthracene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 1.2
Azobenzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Benz(a)anthracene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Benzidine <21 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Benzo(a)pyrene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Benzo(b )fluoranthene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Benzo(g,h,i )perylene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Benzo(k)fluoranthene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Bis(2-chloroethoxy)methane <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Bis(2-chloroethyl) ether <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Bis(2-chloroisopropyl) ether <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Bis(2-ethylhexyl) phthalate <11 19.6 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Butyl benzyl phthalate <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Chrysene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Dibenz(a,h)anthracene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Diethyl phthalate <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Dimethyl phthalate <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Di-n-butyl phthalate <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Di-n-octyl phthalate <11 <10 <10 <10 <10 <10 <10 <10 <10 <8 .57 <10
Fluoranthene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Fluorene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Hexachlorobenzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Hexachlorobutadiene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <28
Hexachlorocyclopentadiene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Hexachloroethane <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <28
lndeno( 1,2,3-cd)pyrene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Isophorone <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Naphthalene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Nitro benzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
N-Nitrosodimethylamine <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
N-Nitrosodi-n-propy lamine <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
N-Nitrosodiphenylamine <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Pentachlorophenol <53 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <50
Phenanthrene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Phenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Pyrene <11 <10 <10 <10 <10 <10 <10 <10 <10 <8.57 <10
Pyridine <11 <10 <10 <10 <10 <10 <10 <10 <10 34.0 <19
Cell4A LDS
Chemical and Radiological Characteristics
Constituent 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019
Major Ions (mg/L)
Carbonate <l <l <l <l <l <l <l <l <l <l <5
Bicarbonate <l <l <l <l <l <l <l <l <l <l <5
Calcium 558 474 470 453 429 336 510 446 542 516 520
Chloride 7570 4670 6040 2710 1910 4200 2860 5200 8610 4360 7360
Fluoride 0.7 39.4 46 27 1970 1320 282 1150 1370 716 1530
Magnesium 6390 3240 5100 2070 1710 2690 2730 3940 4630 3820 3800
Nitrogen-Ammonia 4480 2290 3480 1320 1010 2920 13.4 5050 846 4580 6080
Nitrogen-Nitrate 69 183 94 15 28.9 39 27.4 40.9 63.1 44.0 58.2
Potassium 1960 934 1500 503 305 415 245 675 1710 539 1000
Sodium 12600 6700 11000 3500 2930 4190 3490 8050 11500 6780 13000
Sulfate 92400 41700 77400 39600 31400 56000 50500 91300 89100 68600 72600
pH (s.u.) 1.98 2.53 2.32 2.1 2.32 2.4 2.29 2.04 1.50 1.88 2.39
TDS 117000 56900 93800 55400 49700 81900 65200 95400 142000 75300 112000
Conductivity (umhos/cm) 150000 49000 66600 39600 31300 53600 50200 62200 97900 63400 75600
Metals (ug/L)
Arsenic 133000 54000 74700 44100 35700 51200 10400 43500 117000 42400 52000
Beryllium 536 295 367 180 188 185 199 289 479 298 370
Cadmium 4010 2650 3160 921 1170 4720 4270 4500 4080 3740 1900
Chromium 9140 3890 5940 3930 2630 2780 1760 4250 9410 3930 6500
Cobalt 37300 15200 21700 22300 44300 41200 33700 32100 42700 30600 25000
Copper 222000 116000 150000 481000 754000 439000 160000 331000 650000 376000 500000
Iron 3940000 1420000 2530000 2460000 1370000 1850000 1320000 2330000 5140000 2090000 2500000
Lead 5270 3400 4520 2300 165 991 46.8 797 15500 118 4200
Manganese 389000 157000 207000 95200 86300 98600 96700 184000 296000 136000 190000
Mercury 2.66 6.2 14.7 0.7 <0.5 <0.0020 <0.5 <2.00 <2.00 <2.00 1.4
Molybdenum 49200 23900 29300 10200 1200 3970 278 10700 49900 2350 8400
Nickel 43900 23900 29600 35000 54600 99300 86300 72700 74700 70900 46000
Selenium 5250 2820 3780 1260 1020 2170 649 1590 4940 1550 3100
Silver 204 62 127 44 24.8 <100 25.6 144 312 <100 230
Thallium 252 194 290 332 171 522 218 439 550 281 55
Tin 504 180 119 <100 <100 <17000 <100 <17000 <17000 <17000 <70
Uranium 284000 145000 168000 90200 75000 82200 25000 116000 247000 78600 38000
Vanadium 1150000 518000 770000 240000 157000 510000 253000 449000 1090000 475000 130000
Zinc 298000 152000 204000 181000 163000 306000 510000 502000 385000 446000 210000
Cell4A LDS
Chemical and Radiological Characteristics
Constituent 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019
Radiologies (pCi/L)
17200
Gross Alpha 7020 3230 7440 4730 6930 61800 (8/4/2015) 98700 176000 51000 163000 1670
(5/28/2015)
voes (ug/L)
Acetone 240 130 120 55 57 <700 84.7 61.5 79.8 108 84
Benzene <l <1 <1 <1 <l <5.0 <1 <1 <l <1 <l
Carbon tetrachloride <1 <1 <1 <l <l <5.0 <1 <1 <1 <1 <l
Chloroform 23 52 26 42 110 95 129 84.5 21.6 33.8 31
Chloromethane 7.9 13 3.8 6 9.93 <30.0 5.35 <1.00 3.00 2.41 3.6
MEK 78 50 82 36 <20 <4000 <20 <20 <20 <20 43
Methylene Chloride <1 <1 <1 <1 <1 <5.0 <1 <1 <l 1.05 0.47 J
Naphthalene <l 1.5 <l 1 2.35 <100 <l <l <l <l <l
Tetrahydrofuran 140 158 102 117 39.1 <46.0 18.5 <1 15.7 19.7 16
Toluene <l <l <l <l <l <1000 <l <l <l <1 <l
Xylenes <1 <1 <l <l <1 <10000 <1 <l <l <1 <l
SVOCS (ug/L)
1,2,4-Trichlorobenzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
1,2-Dichlorobenzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
1,3-Dichlorobenzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
1,4-Dichlorobenzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
1-Methy I naphthalene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
2,4,5-Trichlorophenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
2,4,6-Trichlorophenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
2,4-Dichlorophenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
2,4-Dimethylphenol <11 <10 <10 <10 <10 <10 <10 <10 <10 11.1 <10
2,4-Dinitrophenol <54 <20 <20 <20 <20 <20 <20 <10 <10 <9.08 <50
2,4-Dinitrotoluene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
2,6-Dinitrotoluene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
2-Chloronaphthalene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
2-Chlorophenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
2-Methylnaphthalene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
2-Methylphenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
2-Nitrophenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
3&4-Methylphenol <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
3 ,3 '-Dichlorobenzidine <22 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <46
4,6-Dinitro-2-methylphenol <54 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <50
4-Bromophenyl phenyl ether <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
4-Chloro-3-methy lpheno I <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
4-Chlorophenyl phenyl ether <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
4-Nitrophenol <54 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <50
Acenaphthene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Acenaphthylene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Cell4A LDS
Chemical and Radiological Characteristics
Constituent 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019
Anthracene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9 .08 <10
Azobenzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Benz(a)anthracene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Benzidine <22 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Benzo(a)pyrene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Benzo(b )fluoranthene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Benzo(g,h,i)perylene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Benzo(k)fluoranthene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Bis(2-chloroethoxy )methane <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Bis(2-chloroethyl) ether <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Bis(2-chloroisopropyl) ether <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Bis(2-ethylhexyl) phthalate <11 54.9 54.9 16.6 <10 <10 <10 <10 <10 <9.08 1.1
Butyl benzyl phthalate <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Chrysene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Dibenz(a,h)anthracene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Diethyl phthalate <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Dimethyl phthalate <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Di-n-butyl phthalate <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Di-n-octyl phthalate <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Fluoranthene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Fluorene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Hexachlorobenzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Hexachlorobutadiene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <28
Hexachlorocyclopentadiene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Hexachloroethane <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <28
lndeno(l ,2,3-cd)pyrene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Isophorone <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Naphthalene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Nitro benzene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
N-Nitrosodimethy !amine <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
N-Nitrosodi-n-propylamine <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
N-Nitrosodiphenylamine <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Pentachlorophenol <54 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <50
Phenanthrene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Phenol 33 23.5 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Pyrene <11 <10 <10 <10 <10 <10 <10 <10 <10 <9.08 <10
Pyridine <11 <10 <10 <10 <10 <10 <10 <10 <10 12.9 <19
Cell 4B
Chemical and Radiological Characteristics
Constituent 2011 2012 2013 2014 2015 2016 2017 2018 2019
Major Ions (mg/L)
Carbonate <l <l <l <l <l <l <l <l <5
Bicarbonate <l <l <l <l <l <l <l <l <5
Calcium 570 580 662 366 655 523 473 664 670
Chloride 8290 8170 4570 7300 8500 12000 6930 7860 10500
Fluoride 26.7 23.3 1050 1150 1210 1780 1170 1410 2300
Magnesium 3910 4500 3560 3310 5530 5780 3550 5790 6500
Nitrogen-Ammonia 5220 5580 2060 5380 l.09 8690 724 7590 8150
Nitrogen-Nitrate 39 42 51.4 47 15.2 64.5 31.3 42.2 38.6
Potassium 1370 1650 1110 989 1700 1710 1230 1660 1900
Sodium 9050 11700 3150 7100 12800 14100 10600 15700 18000
Sulfate 134000 119000 98100 91500 108000 285000 708000 98400 124000
pH (s.u.) 1.87 1.5 1.65 l.6 1.35 1.26 1.41 1.24 1.53
TDS 98000 128000 108000 131000 149000 172000 103000 117000 180000
Conductivity (umhos/cm) 76900 86900 72800 90100 115000 116000 93800 107000 99600
Metals (ug/L)
Arsenic 67400 80000 65400 70400 106000 139000 82700 97800 140000
Bervllium 311 356 334 275 430 557 347 407 640
Cadmium 1990 2540 1990 2290 2980 4260 2340 2520 2000
Chromium 6860 8280 6390 6940 7450 11900 7800 8630 12000
Cobalt 17800 29300 21300 24600 33700 46700 30300 32900 44000
Copper 193000 340000 340000 368000 499000 684000 457000 539000 830000
Iron 2960000 3580000 2830000 2480000 4340000 6340000 3690000 4400000 5800000
Lead 9960 11600 9820 10900 13400 17900 12200 12500 16000
Manganese 128000 148000 154000 129000 231000 325000 207000 242000 320000
Mercury 13.7 2.6 1.49 <0.0020 1.72 <2.00 <2.00 <2.00 0.46
Molybdenum 21400 27600 26100 29000 39800 55400 22600 27400 29000
Nickel 33900 50500 35100 42000 56400 79600 53000 57800 78000
Selenium 4670 4470 3900 5010 5600 7300 3740 4510 6600
Silver 137 169 137 142 195 307 <100 160 170
Thallium 237 368 243 258 408 559 17.5 33.7 <100
Tin 196 215 163 <17000 211 <17000 <17000 <17000 340
Uranium 133000 171000 110000 133000 200000 278000 23100 28100 36000
Vanadium 660000 783000 163000 666000 881000 868000 746000 828000 710000
Zinc 191000 270000 184000 144000 313000 476000 267000 323000 280000
Cell 4B
Chemical and Radiological Characteristics
Constituent 2011 2012 2013 2014 2015 2016 2017 2018 20.19
Radiologies (pCi/L)
267000
Gross Alpha 8590 13600 14600 148000 (8/4/2015) 42500 262000 132000 320000 310000
(5/28/2015)
voes (ug/L)
Acetone 130 94 43.5 <700 56.2 86.4 38.6 56.8 39
Benzene <l <l <l <5.0 <l <l <l <l <l
Carbon tetrachloride <l <l <I <5.0 <l <l <l <I <I
Chloroform 9.4 4 8.06 <70.0 2.34 3.07 2.39 2.17 3.4
Chloromethane 8.5 8 7.12 <30.0 3.62 6.01 1.26 1.72 2.1
MEK <l <l <20 <4000 <20 <20 <20 27.4 15 J
Methylene Chloride <l <l <l <5.0 <l <l <I <I <l
Naphthalene <l <l <l <100 <l <l <l <I <l
Tetrahydrofuran <10 11.l <l <46.0 <I <l <I 1.87 <35.0
Toluene <I <I <l <1000 <I <l <l <I <l
Xylenes <I <l <l <10000 <l <l <l <I <l
SVOCS (ug/L)
1,2,4-Trichlorobenzene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
1,2-Dichlorobenzene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
l ,3-Dichlorobenzene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
1.4-Dichlorobenzene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
I -Methyl naphthalene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
2.4.5-Trichlorophenol <10 <10 <IO <10 <IO <10 <10 <8.72 <10
2,4,6-Trichlorophenol <10 <10 <10 <10 <10 <10 <10 <8.72 <10
2.4-Dichlorophenol <10 <10 <10 <10 <10 <10 <10 <8.72 <50
2.4-Dimethvlphenol <10 <10 <10 <10 <10 <10 <10 <8.72 <10
2.4-Dinitrophenol <20 <20 <20 <20 <20 <10 <10 <8.72 <10
2.4-Dinitrotoluene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
2.6-Dinitrotoluene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
2-Chloronaphthalene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
2-Chlorophenol <10 <10 <10 <10 <10 <10 <10 <8.72 <10
2-Methylnaphthalene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
2-Methylphenol <10 <10 <10 <10 <10 <10 <10 <8.72 <10
2-Nitrophenol <10 <10 <10 <10 <10 <10 <10 <8 .72 <10
3&4-Methylphenol <10 <10 <10 <10 <10 <10 <10 <8.72 <10
3,3, -Dichlorobenzidine <10 <10 <10 <10 <10 <10 <10 <8.72 <44
4,6-Dinitro-2-methylphenol <10 <10 <10 <10 <IO <10 <10 <8.72 <50
4-Bromophenvl phenyl ether <10 <10 <10 <10 <10 <10 <10 <8.72 <10
4-Chloro-3-methylphenol <10 <10 <10 <10 <10 <10 <10 <8.72 <10
4-Chlorophenvl phenyl ether <10 <10 <10 <10 <10 <10 <10 <8.72 <10
4-Nitrophenol <10 <10 <10 <10 <10 <10 <10 <8.72 <50
Acenaphthene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Acenaphthylene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Anthracene <10 <10 <10 <10 <10 <10 <10 <8.72 1.7
Azobenzene <10 <IO <10 <10 <10 <10 <10 <8 .72 <10
Benz(a)anthracene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Benzidine <10 <10 <10 26 <10 <10 <10 <8.72 <10
Benzo(a)pyrene <10 <10 <IO <10 <10 <10 <10 <8.72 <IO
Benzo(b )fluoranthene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Benzo(g,h,i)perylene <10 <10 <10 <IO <10 <10 <10 <8.72 <10
Cell 4B
Chemical and Radiological Characteristics
Constituent 2011 2012 2013 2014 2015 2016 2017 2018 2019
Benzo(k)fluoranthene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Bis(2-chloroethoxy)methane <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Bis(2-chloroethyl) ether <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Bis(2-chloroisopropyl) ether <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Bis(2-ethylhexyl) phthalate 410 19 <10 <10 <10 <10 <10 <8.72 <10
Butyl benzyl phthalate <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Chrysene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Dibenz(a,h)anthracene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Diethyl phthalate <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Dimethyl phthalate <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Di-n-butyl phthalate <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Di-n-octyl phthalate <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Fluoranthene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Fluorene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Hexachlorobenzene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Hexachlorobutadiene <10 <10 <10 <10 <10 <10 <10 <8.72 <26
Hexachlorocyclopentadiene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Hexachloroethane <10 <10 <10 <10 <10 <10 <10 <8.72 <26
Indeno(l ,2,3-cd)pvrene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Isophorone <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Naphthalene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Nitrobenzene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
N-Nitrosodi me thy !amine <10 <10 <10 <10 <10 <10 <10 <8.72 <10
N-Nitrosodi-n-propylamine <10 <10 <10 <10 <10 <10 <10 <8.72 <10
N-Nitrosodi phen ylamine <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Pentachlorophenol <10 <10 <10 <10 <10 <10 <10 <8.72 <50
Phenanthrene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Phenol <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Pyrene <10 <10 <10 <10 <10 <10 <10 <8.72 <10
Pyridine <10 <10 <10 15 <10 <10 <10 31.7 <18
Cell4B LDS
Chemical and Radiological Characteristics
Constituent 2011 2012 2013 2014 2015 2016 2017 2018 2019
Major Ions (mg/L)
Carbonate <1 <l dry <1 <l <l <l <1 <5
Bicarbonate <1 <1 dry <1 <l <1 <1 <1 <5
Calcium 486 456 dry 308 538 547 516 592 550
Chloride 3630 6850 dry 6900 7960 8510 10400 8060 8050
Fluoride 28.4 22 dry 970 1150 1290 1050 1480 1680
Magnesium 3230 3360 dry 3400 5190 4780 5370 5580 4800
Nitrogen-Ammonia 4260 4090 dry 5240 2.43 7540 739 7510 7080
Nitrogen-Nitrate 30 31 dry 43 16.6 49.6 63.9 47.4 41.2
Potassium 1130 1060 dry 952 1560 1360 2130 1620 1400
Sodium 8240 8080 dry 6920 11900 10800 13200 14500 13000
Sulfate 59900 99100 dry 82300 104000 163000 117000 100000 89500
pH (s.u.) 2.23 2.4 dry 2.2 1.51 1.88 1.44 1.35 1.73
TDS 85800 90200 dry 129000 131000 133000 168000 132000 131000
Conductivity (umhos/cm) 63000 62400 dry 76300 106000 68400 105000 104000 80800
Metals (ug/L)
Arsenic 54200 41200 dry 67800 98400 98800 135000 94100 89000
Beryllium 274 271 dry 282 411 430 559 416 470
Cadmium 1670 1740 dry 2290 2790 3250 4500 2610 2000
Chromium 6250 5930 dry 6160 7320 9470 13700 8980 9100
Cobalt 15600 19000 dry 23300 31100 33600 48900 31700 31000
Copper 176000 181000 dry 308000 458000 475000 681000 497000 550000
Iron 2450000 2120000 dry 2590000 4180000 4680000 5910000 4190000 4400000
Lead 6060 4420 dry 4120 10100 5860 14000 8770 7800
Manganese 118000 162000 dry 144000 222000 262000 346000 239000 240000
Mercury 12.3 3 dry 0.002 1.47 <2.00 <2.00 <2.00 0.1 lJ
Molybdenum 16700 15000 dry 24300 36300 35500 52900 25900 27000
Nickel 30700 33700 dry 40100 52600 58100 84400 56100 59000
Selenium 3710 2880 dry 4080 5080 5310 6860 4500 4700
Silver 111 117 dry 119 179 224 266 156 170
Thallium 179 175 dry 336 354 414 427 245 87
Tin 332 <100 dry <17000 198 <17000 <17000 <17000 200
Uranium 111000 132000 dry 143000 185000 192000 269000 54200 31000
Vanadium 518000 428000 dry 671000 817000 847000 1260000 811000 760000
Zinc 172000 182000 dry 144000 296000 315000 443000 303000 280000
Cell 4B LDS
Chemical and Radiological Characteristics
Constituent 2011 2012 2013 2014 2015 2016 2017 2018 2019
Raaiologics (pGi/L)
375000
Gross Alpha 6000 7500 dry 181000 (8/4/2015) 185000 165000 305000 226000 52500
(5/28/2015)
voes (ug/L)
Acetone 390 370 d(Y <700 218 266 479 147 102
Benzene <l <l dry <5.0 <l <l <1 <l <1
Carbon tetrachloride <l <l dry <5.0 <l <l <l <l <l
Chloroform 20 19 dry <70.0 5.03 9.97 9.13 4.74 3.9
Chloromethane 11 11 dry <30.0 9.72 10.8 7.16 2.4 2.3
MEK 240 180 dry <4000 71.8 53.6 89.4 34.6 71
Methylene Chloride <1 <l dry <5.0 <l <1 1.01 <l <1
Naphthalene <l <l dry <100 <l <1 <l <l <l
Tetrahydrofuran 198 322 dry 75.6 36.6 75.9 51.2 17.3 53
Toluene <l <l dry <1000 <l <l <l <l <l
Xylenes <l <l dry <10000 <l <l <1 <l <1
SVOCS (ug/L)
1,2,4-Trichlorobenzene <10 <10 dry <10 <10 <10 <10 <8.79 <10
1,2-Dichlorobenzene <10 <10 dry <10 <10 <10 <10 <8.79 <10
1,3-Dichlorobenzene <10 <10 dry <10 <10 <10 <10 <8.79 <10
1,4-Dichlorobenzene <10 <10 dry <10 <10 <10 <10 <8.79 <10
1-Methylnaphthalene <10 <10 dry <10 <10 <10 <10 <8.79 <10
2,4,5-Trichlorophenol <10 <10 dry <10 <10 <10 <10 <8.79 <10
2,4,6-Trichlorophenol <10 <10 dry <10 <10 <10 <10 <8.79 <10
2,4-Dichlorophenol <10 <10 dry <10 <10 <10 <10 <8.79 <10
2,4-Dimethylphenol <10 <10 dry <10 <10 <10 <10 <8.79 <10
2,4-Dinitrophenol <20 <20 dry <20 <20 <20 <10 <8.79 <50
2,4-Dinitrotoluene <10 <10 dry <10 <10 <10 <10 <8.79 <10
2,6-Dinitrotoluene <10 <10 dry <10 <10 <10 <10 <8.79 <10
2-Chloronaphthalene <10 <10 dry <10 <10 <10 <10 <8.79 <10
2-Chlorophenol <10 <10 dry <10 <10 <10 <10 <8.79 <10
2-Methy !naphthalene <10 <10 dry <10 <10 <10 <10 <8.79 <10
2-Methylphenol <10 <10 dry <10 <10 <10 <10 <8.79 <10
2-Nitrophenol <10 <10 dry <10 <10 <10 <10 <8.79 <10
3&4-Methylphenol <10 <10 dry <10 <10 <10 <10 <8.79 0.42
3,3 '-Dichlorobenzidine <10 <10 dry <10 <10 <10 <10 <8.79 <45
4,6-Dinitro-2-methylphenol <10 <10 dry <10 <10 <10 <10 <8.79 <50
4-Bromophenyl phenyl ether <10 <10 dry <10 <10 <10 <10 <8.79 <10
4-Chloro-3-methylphenol <10 <10 dry <10 <10 <10 <10 <8.79 <10
4-Chlorophenyl phenyl ether <10 <10 dry <10 <10 <10 <10 <8.79 <10
4-Nitrophenol <10 <10 dry <10 <10 <10 <10 <8.79 <50
Acenaphthene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Acenaphthylene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Cell4B LDS
Chemical and Radiological Characteristics
Constituent 2011 2012 2013 2014 2015 2016 2017 2018 2019
Anthracene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Azobenzene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Benz(a)anthracene <10 <10 drv <10 <10 <10 <10 <8.79 <10
Benzidine <10 <10 dry <10 <10 <10 <10 <8.79 <10
Benzo(a)pyrene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Benzo(b )fluoranthene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Benzo(g,h,i)perylene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Benzo(k)fluoranthene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Bis(2-chloroethoxy)methane <10 <10 dry <10 <10 <10 <10 <8.79 <10
Bis(2-chloroethyl) ether <10 <10 dry <10 <10 <10 <10 <8.79 <10
Bis(2-chloroisopropyl) ether <10 <10 dry <10 <10 <10 <10 <8.79 <10
Bis(2-ethylhexyl) phthalate 191 191 dry 27 <10 132 145 65.9 16
Butyl benzyl phthalate <10 <10 dry <10 <10 <10 <10 <8.79 <10
Chrysene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Dibenz(a,h)anthracene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Diethyl phthalate <10 <10 dry <10 <10 <10 <10 <8.79 <10
Dimethyl phthalate <10 <10 dry <10 <10 <10 <10 <8.79 <10
Di-n-butyl phthalate <10 <10 dry <10 <10 <10 <10 <8.79 <10
Di-n-octyl phthalate <10 <10 dry <10 <10 <10 <10 <8.79 <10
Fluoranthene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Fluorene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Hexachlorobenzene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Hexachlorobutadiene <10 <10 dry <10 <10 <10 <10 <8.79 <27
Hexachlorocyclopentadiene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Hexachloroethane <10 <10 dry <10 <10 <10 <10 <8.79 <27
lndeno( 1,2,3-cd)pyrene <10 <10 drv <10 <10 <10 <10 <8.79 <10
Isophorone <10 <10 dry <10 <10 <10 <10 <8.79 <10
Naphthalene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Nitro benzene <10 <10 dry <10 <10 <10 <10 <8.79 <10
N-Nitrosodimethylamine <10 <10 dry <10 <10 <10 <10 <8.79 <10
N-Nitrosodi-n-propylamine <10 <10 dry <10 <10 <10 <10 <8.79 <10
N-Nitrosodiphenylamine <10 <10 dry <10 <10 <10 <10 <8.79 <10
Pentachlorophenol <10 <10 dry <10 <10 <10 <10 <8.79 <50
Phenanthrene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Phenol <10 <10 dry <10 <10 <10 <10 <8.79 <10
Pyrene <10 <10 dry <10 <10 <10 <10 <8.79 <10
Pyridine <10 <10 dry <10 <10 <10 <10 29.1 <18
Cell 1
Additional Radiological Analyses
Thorium-228 Thorium-230 Thorium-232 Radium-226 Uranium-233/234 Uranium-235/236 Uranium-238 Specific Gravity (oCi/L) (oCi/L) (oCi/L) (oCi/L) (oCi/L) (oCi/L) <oCi/L)
8/4/15 1310 991000 6150 1110 141000 8920 140000 1.21
5/28/15 204 782000 6730 829 96700 5980 100000 1.13
8/30/16 ND 677000 4480 497 2380 45800 1.15
8/29/17 2890 8100000 76000 391 353000 20400 344000 1.17
8/1/18 ND 856000 8410 443 97300 6970 97200 1.16
8/21/19 1380 747000 4780 348 28400 1650 28700 1.15
8/21/2019
(Cell 65 -1500 663000 5720 434 25500 1960 27700 1.15 Duplicate
of Cell 1)
Thorium-228 Thorium-230
(pCi/L) (pCi/L)
8/4/15 ND 6680
8/30/16 ND 5050
8/29/17 ND 38500
8/1/2018 ND 7390
8/1/2018
(cell 65 -
Duplicate ND 6860
of Cell 2
Slimes)
8/21/2019 ND 1750
Cell 2 Slimes Drain
Additional Radiological Analyses
Thorium-232 Radium-226 Uranium-
(pCi/L) (pCi/L) 233/234 (pCi/L)
ND 36.6 11300
ND 52.4 11700
ND 51.2 111000
ND 36.2 14900
ND 29.8 10700
ND 62.5 9300
Uranium-Uranium-238 Specific Gravity 235/236 (pCi/L) (pCi/L)
858 10500 1.09
599 10700 1.03
ND 75600 1.07
ND 12500 1.07
3440 12600 1.06
484 9150 1.03
Cell 3
1tmna a 10 ogaca na yses Add' ' IR d" l . I A I
Thorium-228 Thorium-230 Thorium-232 Radium-226 Uranium-Uranium-Uranium-238 Specific Gravity (pCi/L) (pCi/L) (pCi/L) (pCi/L) 233/234 (pCi/L) 235/236 (pCi/L) (pCi/L)
8/4/15 ND 123000 1640 448 184000 10300 191000 1.21
5/28/15 798 131000 1290 202 557000 37900 591000 1.29
8/30/16 983 72500 1670 584 1960000 130000 2060000 1.62
1S/.5Ufl0
(cell 65 -ND 67000 788 640 2520000 130000 2490000 1.53 Duplicate
of Cell 3)
8/29/17 ND ND ND 101 37600 ND 32800 0.989
8/1/18 ND 28100 2310 79.8 398000 24000 468000 1.21
8/21/19 ND 6610 ND 48.0 6640 ND 5780 1.07
Cell 4A
Additional Radiological Analyses
Thorium-228 Thorium-230 Thorium-232 Radium-226 Uranium-Uranium-Uranium-238 Specific Gravity (oCi/L) (oCi/L) (oCi/L) (oCi/L) 233/234 ( oCi/L) 235/236 (oCi/L) (oCi/L)
8/4/15 ND 374000 3490 663 57500 3720 64400 1.11
5/28/15 327 405000 3440 ND 61200 4030 62700 1.07
5/28/2015
(Cell 65 -
Duplicate 265 315000 3790 772 58600 3020 58300 NS
of Cell
4A)
8/30/16 ND 466000 2870 1050 61100 3320 70900 1.10
8/29/17 ND 4450000 47700 759 637000 30600 692000 1.09
8/29/17
(Cell 65 -
Duplicate ND 4080000 11000 822 602000 44900 616000 1.12
of Cell
4A)
8/1/18 1970 539000 8230 59.2 88700 9900 86300 1.10
8/21/19 941 430000 2870 260 9350 674 10900 1.02
Thorium-228 Thorium-230
(pCi/L) (pCi/L)
8/4/15 ND 25300
5/28/15 ND 25300
8/30/16 ND 134000
8/29/17 ND 5410000
8/1/18 ND 76000
8/21/19 1060 366000
Cell 4A LDS
Additional Radiological Analyses
Thorium-232 Radium-226 Uranium-
(pCi/L) (pCi/L) 233/234 (pCi/L)
ND 19.3 9380
ND 19.3 9380
1130 51.1 46200
49200 286 852000
ND 38.2 28800
2230 73.4 13500
Uranium-Uranium-238 Specific Gravity 235/236 (pCi/L) (pCi/L)
504 10800 1.07
504 10800 NS
1900 40400 1.10
66200 851000 1.17
ND 30500 1.05
738 13000 1.02
Cell 4B
Additional Radiological Analyse
Thorium-228 Thorium-230 Thorium-232 Radium-226 Uranium-233/234 Uranium-235/236 Uranium-238 Specific Gravity (pCi/L) (oCi/L) (oCi/L) (pCi/L) (oCi/L) (oCi/L) (pCi/L)
8/4/15 ND 410000 2210 611 63500 3710 67000 1.12
5/28/15 122 346000 3790 544 65000 3870 66100 1.08
8/30/16 ND 595000 3510 715 90200 4090 90100 1.13
8/29/17 ND 3390000 56000 489 76000 8100 92700 1.07
8/1/18 ND 461000 7360 307 13700 ND 8420 1.08
8/21/19 1080 434000 3490 296 11600 563 10800 1.10
Thorium-228 Thorium-230
(nCi/L) (pCi/L)
8/4/15 ND 452000
8/4/15
(Cell 65 -
Duplicate ND 436000
ofCell 4B
LOS)
5/28/15 334 487000
8/30/16 ND 368000
8/29/17 4680 5220000
8/1/18 1520 424000
8/21/19 1030 368000
Cell 4B LDS
Additional Radiological Analyses
Thorium-232 Radium-226 Uranium-
(nCi/L) (oCi/L) 233/234 (nCi/L)
3660 161 62600
4000 125 62600
5430 55.2 63500
1010 104 78600
43200 143 846000
5130 88.3 14300
2650 105 8840
Uranium-235/236 Uranium-238 Specific Gravity (pCi/L) (oCi/L)
3890 60900 1.12
2680 61300 1.12
3900 65500 NS
3820 78900 1.11
64200 894000 1.07
ND 18400 1.09
412 9600 1.05
TabE
Quality Assurance and Data Validation Tables
Table E-1 Holding Time Evaluation**
I ~i.;,J} l Cell '! Ollll .l' OJliQ ·te~l4~ 1611 .IB ~IM1Sil ·~'IJ .
R~r,l\11tl 0 !Win.., 'll't1n;,., $0 1t1 !Im linm ~c,t 'i~[UCI@l'iJ I ~ ~'llflilns ··B (CCU l) Drain
Carbonate 14 days OK OK OK OK OK OK OK OK
Bicarbonate 14 days OK OK OK OK OK OK OK OK
Calcium 6 months OK OK OK OK OK OK OK OK
Chloride 28 days OK OK OK OK OK OK OK OK
Fluoride 28 days OK *** OK OK OK OK OK OK
Magnesium 6 months OK OK OK OK OK OK OK OK
Nitrogen-Ammonia 28 days OK OK OK OK OK OK OK OK
Nitrogen-Nitrate 28 days OK OK OK OK OK OK OK OK
Potassium 6 months OK OK OK OK OK OK OK OK
Sodium 6 months OK OK OK OK OK OK OK OK
Sulfate 28 days OK OK OK OK OK OK OK OK
pH (pH units) Immediately OK* OK* OK* OK* OK* OK* OK* OK*
TDS 7 days OK OK OK OK OK OK OK OK
Conductivity (umhos/cm) NIA OK OK OK OK OK OK OK OK
6 months (except
mercury which is 28
Metals days) OK OK OK OK OK OK OK OK
Radiologies 6 months OK OK OK OK OK OK OK OK
VOCS (including THF) 14 days OK OK*** OK OK OK OK OK OK
7 days to extractton/40
svocs days for analysis *** *** *** *** *** *** *** ***
* Per the method, pH should be analyzed within 15 minutes of sample collection. Due to the nature of the solution matrix, sample handling in the
field is minimized and pH is measured by the laboratory upon receipt. This procedure change was requested by and approved by DWMRC.
** -The voluntary analyses conducted for specific gravity, thorium isotopes, uranium isotopes, and radium-226 are for informational purposes only.
These analyses do not have QAP required holding times, and therefore, are not included in the holding time evaluation.
*** Hold times were exceeded as noted in Section 4.3.2 of the text
E-2 Laboratory Receipt Temperature Check
Wor-k @raer Number/Lab
Set ID Receipt Temp
GEL-488668 NIA
EL -C19081073 OK*
NI A = These shipments contained samples for the analysis of
radionuclides only. Samples submitted for radionuclide
analyses do not have a sample temperature requirement.
*The samples were received at EL from the Mill at <6.0°C. As
noted in the text, Section 4.3.3, when EL shipped the SVOCs to
the subcontract lab, 4 samples were received at 7 .6°C.
E-3: Analytical Method Check -Routine Samples**
Parameter QAP/Permit Method Method Used by Lab
Ammonia (as N) A4500-NH3 G or E350.1 E350.l
Nitrate+ Nitrite (as N) E353.1 or E353.2 E353.2
Metals E200.7 or E200.8 (Hg 245.1) E200.7 and E200.8 and 245.1 (Hg)
Gross Alpha E900.0 or E900.1 or E903.0 E903.0
voes SW8260B or SW8260C SW8260C
Chloride A4500-Cl B or E300.0 E300.0
Fluoride A4500-F C or E300.0 E300.0
Sulfate A4500-S04 E or E300.0 E300.0
TDS A2540 C SM2540C
Carbonate as C03, Bicarbonate as HC03 A2320 B SM2320B
pH Not Specified SW9040C
Conductivity Not Specified SM25IOB
SVOCs SW8270D SW8270C .. . -' ·•* -The voluntary analy es condu ted l·or pecJfic gravity, 1honum I oLopes, urarnum isotopes and rad,um-226 are tor
informational purposes only. These analyses do not have QAP required methods, and therefore, are not included in the
analytical method evaluation.
E-4 Reporting Limit Evaluation**
Parameter Permit-Specified RL
Ammonia (as N) 25 mg/L
Nitrate + Nitrite (as N) 10 mg/L
Metals ug/L
Arsenic 50
Beryllium 4
Cadmium 5
Chromium 100
Cobalt 730
Copper 1300
Iron 11000
Lead 15
Manganese 800
Mercury 2
Molybdenum 40
Nickel 100
Selenium 50
Silver 100
Thallium 2
Tin 17000
Uranium 30
Vanadium 60
Zinc 5000
Gross Alpha 15
voes ug/L
Acetone 700
Benzene 5
Carbon tetrachloride 5
Chloroform 70
Chloromethane 30
MEK 4000
Methylene Chloride 5
Naphthalene 100
. Tetrahydrofuran 46
• a •-Toluene 1000
Xylenes 10000
Major Ions
Chloride 1.0 mg/L
Fluoride 4mg/L
Sulfate 1000 mg/L
TDS 1000 mg/L
Carbonate as C03, Bicarbonate as HC03 *
Calcium, Magnesium, Potassium, Sodium *
SVOCs (from the 8270D LLD) ug/L
1,2,4-Trichlorobenzene 10
1,2-Dichlorobenzene 10
E-4 Reporting Limit Evaluation**
Parameter Permit-Specified RL
1,3-Dichlorobenzene IO
1,4-Dichlorobenzene 10
1-Methylnaphthalene 10
2,4,5-Trichlorophenol IO
2,4,6-Trichlorophenol IO
2,4-Dichlorophenol 10
2,4-Dimethy !phenol 10
2,4-Dinitrophenol 50
2,4-Dinitrotoluene 10
2,6-Dinitrotoluene 10
2-Chloronaphthalene 10
2-Chlorophenol IO
2-Methy !naphthalene 10
2-Methylphenol IO
2-Nitrophenol 10
3&4-Methylphenol 10
3 ,3 , -Dichlorobenzidine 20
4,6-Dinitro-2-methylphenol 50
4-Bromophenyl phenyl ether IO
4-Chloro-3-methylphenol 20
4-Chlorophenyl phenyl ether 10
4-Nitrophenol 50
Acenaphthene 10
Acenaphthylene 10
Anthracene IO
Azobenzene *
Benz( a)anthracene 10
Benzi dine *
Benzo( a)pyrene 10
Benzo(b )fluoranthene 10
Benzo(g,h,i )pery lene IO
Benzo(k)fluoranthene 10
B is(2-chloroethoxy )methane 10
Bis(2-chloroethyl) ether 10
Bis(2-chloroisopropyl) ether 10
Bis(2-ethylhexyl) phthalate *
Butyl benzyl phthalate 10
Chrysene 10
Dibenz( a,h)anthracene 10
Diethyl phthalate 10
Dimethyl phthalate 10
Di-n-butyl phthalate 10
Di-n-octyl phthalate IO
Fluoranthene 10
Fluorene 10
E-4 Reporting Limit Evaluation**
Parameter Pe..rmit-Spe,dfied RL
Hexachlorobenzene 10
Hexachlorobutadiene 10
Hexachlorocyclopentadiene 10
Hexachloroethane 10
Indeno( 1,2,3-cd)pyrene 10
Isophorone 10
Naphthalene 10
Nitro benzene 10
N-Nitrosodimethylamine *
N-Nitrosodi-n-propylamine 10
N-Nitrosodiphenylamine 10
Pentachlorophenol 50
Phenanthrene 10
Phenol 10
Pyrene 10
Pyridine *
All analyses were reported to the required RLs unless noted in the text.
* Reporting limits for these analytes are not specified in either the Permit
or EPA Method 8270D. The reporting limits established by the laboratory
are reported here. The reporting limits are comparable to other analytes in
the same method based on the matrix.
** -The voluntary analyses conducted for specific gravity, thorium isotopes, uranium
isotopes, and radium-226 are for informational purposes only. These analyses do not
have QAP required reporting limits, and therefore, are not included in the reporting
limit evaluation.
E-5: Trip Blank Evaluation
All trip blanks for the 2019 sampling program were nondetect.
Blank Sample Date Laboratory
1 8/21/2019 EL
-U.PIIC!lte E6D r amp e e ahve s I R I . P ercent I erence"' · D'ff "*
Major Ions (mg/I) Cell I Cell 65 RPO%
Carbonate <S <S NC
Bicarbonate <S <S NC
Calcium 720 620 14.9
Chloride 19800 19300 2.6
Fluoride 3480 2980 15.S
Magnesium 9200 7000 27.2
Nitrogen-Ammonia 10400 12000 14.3
Nitrogen-Nitrate 118 114 3.4
Potassium 2600 1900 31.1
Sodium 28000 21000 28.6
Sulfate 169000 169000 0.0
pH (s.u.) 1.14 1.13 0.9
TDS 257000 255000 0.8
Conductivity (umhos/cm) 119000 118000 0.8
Metals (mg/I)
Arsenic 270 230 16.0
Beryllium 0.93 0.90 3.3
Cadmium S.4 4.8 11.8
Chromium IS 12 22.2
Cobalt 66 60 9.5
Copper 1700 1500 12.5
Iron 9100 7800 15.4
Lead 22 22 0.0
Manganese 540 470 13.9
Mercury 0.0037 0.0032 14.5
Molybdenum 120 110 8.7
Nickel 110 90 20.0
Selenium 10 7.9 23.5
Silver 0.79 0.69 13.5
Thallium <700 0.13 NC
Tin 0.54 0.46 16.0
Uranium 81 77 5.1
Vanadium 1400 1300 7.4
Zinc 550 490 11.S
Radiololtics (pCi/1)
Gross Alpha* 326000 398000 17.9
voes (u!!.11.)
Acetone 28 30 6.9
Benzene <1.0 <1.0 NC
Carbon tetrachloride <1.0 <1.0 NC
Chloroform 7.5 6.9 8.3
Chloromethane 2.3 2.4 4.3
MEK II 10 9.S
Methylene Chloride <1.0 <1.0 NC
Naphthalene <1.0 <1.0 NC
Tetrahydrofuran <35.0 <35.0 NC
Toluene <1.0 <1.0 NC
Xylenes <1.0 <1.0 NC
SVOCS (u!!/1 )
1,2,4-Trichlorobenzene <10 <10 NC
1,2-Dichlorobenzene <10 <10 NC
1,3-Dichlorobenzene <10 <IO NC
1,4-Dichlorobenzene <10 <10 NC
1-Methvlnaphthalene <10 <10 NC
2,4,5-Trichlorophenol <10 <10 NC
2,4,6-Trichlorophenol <10 <10 NC
2,4-Dichlorophenol <10 <10 NC
2,4-Dimethylphenol <10 <10 NC
2,4-Dinitrophenol <50 <50 NC
2,4-Dinitrotoluene <10 <10 NC
2,6-Dinitrotoluene <10 <10 NC
E-6 Duplicate Sample Relative Percent Difference**
Major Ions (mg/I) Cell I Cell 65 RPO%
2-Chloronaphthalene <10 <10 NC
2-Chlorophenol <10 <10 NC
2-Methylnaphthalene <10 <10 NC
2-Methy]phenol <10 <10 NC
2-Nitrophenol <10 <10 NC
3&4-Methylphenol <10 <10 NC
3,3 '-Dichlorobenzidine <50 <49 NC
4,6-Dinitro-2-methylphenol <50 <50 NC
4-Bromophenyl phenyl ether <10 <10 NC
4-Chloro-3-methylphenol <10 <10 NC
4-Chlorophenyl phenyl ether <10 <10 NC
4-Nitrophenol <50 <50 NC
Acenaphthene <10 <10 NC
Acenaphthy]ene <10 <10 NC
Anthracene <10 <10 NC
Azobenzene <10 <10 NC
Benz(a)anthracene <10 <10 NC
Benzidine <100 <10 NC
Benzo(a)pyrene <10 <10 NC
Benzo(b )fluoranthene <10 <10 NC
Benzo(11.,h,i)pervlene <10 <10 NC
Benzo(k)fluoranthene <10 <10 NC
Bis(2-chloroethoxv)methane <10 <10 NC
Bis(2-chloroethvl) ether <10 <10 NC
Bis(2-chloroisopropy]) ether <10 <10 NC
Bis(2-ethylhexvl) phthalate <10 <10 NC
Butyl benzyl phthalate <10 <10 NC
Chrysene <10 <10 NC
Dibenz(a,h)anthracene <10 <10 NC
Diethyl phthalate <10 <10 NC
Dimethyl phthalate <10 <10 NC
Di-n-butyl phthalate <10 <10 NC
Di-n-octyl phthalate <10 <10 NC
Fluoranthene <10 <10 NC
Fluorene <10 <10 NC
Hexachlorobenzene <10 <10 NC
Hexachlorobutadiene <30 <30 NC
Hexachlorocyclopentadiene <10 <10 NC
Hexachloroethane <30 <30 NC
Indeno( 1,2,3-cd)pyrene <10 <10 NC
Isophorone <10 <10 NC
Naphthalene <10 <10 NC
Nitrobenzene <10 <10 NC
N-Nitrosodimethylamine <10 <10 NC
N-Nitrosodi-n-propylamine <10 <10 NC
N-Nitrosodiphenylamine <10 <10 NC
Pentachlorophenol <50 <50 NC
Phenanthrene <10 <10 NC
Phenol <10 <10 NC
Pyrene <10 <10 NC
Pyridine <20 <20 NC
Highlighted cells indicate an RPO that exceeded the 20% RPO criteria
Per the approved QAP, an RPD greater than 20% is acceptable if the reported results are less than 5 times the RL. These results are
provided for information only.
* Duplicate checks reported for gross alpha minus RN and U are not %RPO. Calculated values are based on the formula in the approved
QAP.
** -The voluntary analyses conducted for specific gravity, thorium isotopes, uranium isotopes, and radium-226 are for informational
purposes only. These analyses do not have QAP required duplicate requirements, and therefore, are not included in the duplicate
evaluation.
E-7 Radiologies Counting Error
a~ OS" Aljplirn I
1~010 l!I•, 'Rilil &. Q , u11i,1l1ili.ig
CG,ttil M')nta . t: 'P,.1 e~-~ A1 •~ I &•,rs ,ifuiun
Sample, [D) mniJmirB, • II U (tj I '.Z& GWQS GWQS
Cell 1 326000 2590 y 15 NA
Cell 2 Slimes 3790 302 y 15 NA
Cell 3 3890 302 y 15 NA
Cell 4A 261000 2840 y 15 NA
Cell4ALDS 163000 1990 y 15 NA
Cell 4B 310000 3100 y 15 NA
Cell4B LDS 226000 2230 y 15 NA
Cell 65 (Duplicate of Cell 1) 398000 3070 y 15 NA
GWQS = Groundwater Quality Standard
E-8: Laboratory Matrix QC
Matrix Spike % Recovery Comparison
Lab Report Sample ID
19081073 Cell 4A
NC= Not Calculated
LCS % Recovery
Lab Report Analyte
19081073 1,2,4,-Trichlorobenzene
19081073 1,2,-Dichlorobenzene
19081073 1,3,-Dichlorobenzene
19081073 1,4,-Dichlorobenzene
19081073 Hexachlorobutadiene
19081073 Indene
LCSD % Recovery
Lab Report Analyte
19081073 1,1 '-Biphenyl
19081073 1,2,4,5,-Tetrachlorobenzene
19081073 1,2,4,-Trichlorobenzene
19081073 1,2,-Dichlorobenzene
19081073 1,3, -Dich lorobenzene
19081073 1,4,-Dichlorobenzene
19081073 2-Chloronaphthalene
19081073 2-Methylnaphthalene
19081073 Acenaphthylene
19081073 Hexachlorobutadiene
19081073 Hexachloroethane
19081073 Naphthalene
19081073 1-Methylnaphthalene
19081073 Pyridine
19081073 Indene
Surrogate % Recovery
Lab Report Well/Sample
19081073 Cell 1
19081073 Cell I
19081073 Cell I
19081073 Cell I
19081073 Cell 4A
19081073 Cell 4B
19081073 Cell 4B
19081073 Cell 65 (Duplicate of Cell 1)
19081073 Cell 65 (Duplicate of Cell I)
19081073 Cell 65 (Duplicate of Cell 1)
MSD
Analyte MS %REC %REC REC Range RPD
TDS 20 NIA 90 -110 NC
LCS %REC REC Range
41 47 -103
43 44-103
39 42 -100
40 43 -101
34 41 -102
45 46-108
LCSD %REC REC Range
49 53 -116
42 • 52 -100
32 47 -103
35 44-103
31 42 -100
33 43 -101
45 52 -116
44 55 -101
57 58 -112
25 41 -102
25 31 -100
46 53 -105
46 57 -100
22 10 -69
38 46 -108
Lab
Surrogate Specified
Analyte %REC REC Range
2,4,6-Tribromophenol 34 52 -123
2-Fluorobiphenyl 26 47 -119
Nitrobenzene-d5 36 45 -113
Terphenyl-dl4 27 50 -123
Terphenyl-d14 31 50 -123
2-Fluorobiphenyl 41 47 -119
Terphenyl-d14 31 50 -123
2,4,6-Tribromophenol 46 52 -123
2-Fluorobiphenyl 32 47 -119
Terphenyl-d 14 32 50 -123
E-8: Laboratory Matrix QC
Labora tory Duplicate % Recovery Comparison
Cab
Duplicate UJl'Jj) Ra11 r~
Lat, U,epo:r.t 'Well I ~u~~fe ~'itmple 1Jl1~4Jiu) t J.ti:sult .(t!,pf.j ~ %
488668 Cell 3 Gross Alpha 3890 5400 32.6 0-20
Method Blanks
, ~b n ,ctp t11 W«lll Am~lr ll!-ntank: Ri.Lciutl Q6
19081073 NA Sulfate 0.20 mg/L