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HomeMy WebLinkAboutDRC-2017-001602 - 0901a068806c7164Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www.energyfuels.com February 27, 2017 VIA OVERNIGHT DELIVERY Mr. Scott Anderson Director Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144880 Salt Lake City, UT 84114-4820 Mr. Anderson: Div ot MfiPggsfflent and imiifliisn Control FEB 2 8 201? 'm-mi-oouz- Re: State of Utah Radioactive Material License No. UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period July 1 through December 31, 2016 As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65 (subpartl)), and License Condition 11.3A of State of Utah Radioactive Materials License No. UT1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill for the period July 1 through December 31, 2016. If you have any questions regarding this report, please contact the undersigned at (303) 389- 4134. Yours very, truly, Energy Fuels Resources (USA) Inc. Kathy Weinel Quality Assurance Manager cc: David C. Frydenlund Mark Chalmers David E. Turk Scott A. Bakken Logan Shumway February 27,2017 VIA OVERNIGHT DELIVERY Mr. Scott Anderson Director Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144880 Salt Lake City, UT 84114-4820 Mr. Anderson: Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www .energyfuels.com Re: State of Utah Radioactive Material License No. UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period July 1 through December 31,2016 As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65 (subpartl)), and License Condition 11.3A of State of Utah Radioactive Materials License No. UT1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill for the period July 1 through December 31, 2016. If you have any questions regarding this report, please contact the undersigned at (303) 389- 4134. ~:;:r2J ENERGY FUELS RESOURCES (USA) INC. Kathy Weinel Quality Assurance Manager cc: David C. Frydenlund Mark Chalmers David E. Turk Scott A. Bakken Logan Shumway White Mesa Uranium Mill Radioactive Materials License UT900479 Semi-Annual Effluent MoQitoring Report (July through December 2016) Prepared For: Utah Department of Environmental Quality Division of Waste Management and Radiation Control Prepared by: Energy Fuels Resources (USA) Inc. 225 Union Boulevard, Suite 600 Lakewood, CO 80228 February 27,2017 TABLE OF CONTENTS 1.0 INTRODUCTION .................................................................................................. 1 1.1 Modifications to the Monitoring Programs ............................................................... 1 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING ..................................... 3 2.1 Program Overview ............................................................................................... 3 2.2 Sampling Protocol and Analytical Results ........................................................... 3 2.3 General Observations ........................................................................................... 5 2.4 Site Specific Sampling Data ................................................................................. 5 2.5 Radon-222 ............................................................................................................ 6 3.0 EXTERNAL RADIATION (DIRECT GAMMA) .................................................. 7 4.0 VEGETATION SAMPLES ..................................................................................... 7 5.0 STACK SAMPLING ............................................................................................... 8 6.0 SURFACE WATER MONITORING ...................................................................... 9 7.0 SOIL SAMPLING ................................................................................................. 10 8.0 METEOROLOGICAL MONITORING ................................................................ 10 9.0 CELL 2 RADON FLUX ........................................................................................ 10 10.0 SIGNATURE AND CERTIFICATION ................................................................ 12 LIST OF TABLES Table 1 NCRP Report 94-Global Pb-210 Concentration Example Table 2 Air Monitoring Station Results U-Nat (Comparison to Limits) Table 3 Air Monitoring Station Results Th-230 (Comparison to Limits) Table 4 Air Monitoring Station Results Ra-226 (Comparison to Limits) Table 5 Air Monitoring Station Results Pb-210 (Comparison to Limits) Table 6 Air Monitoring Station Results Th-232 (Comparison to Limits) Table 7 Environmental OSL Dosimeter Measurements (Gamma) Table 8 Stack Effluent Concentrations and Release Rates 1 INDEX OF TABS A High Volume Air Monitoring Stations B BHV Air Sampling Graphs and Data Tables Tab 1 BHV -1 Air Sampling Graphs and Data Table Tab 2 BHV-2 Air Sampling Graphs and Data Table Tab 3 BHV -3 Air Sampling Graphs and Data Table Tab 4 BHV -4 Air Sampling Graphs and Data Table Tab 5 BHV -5 Air Sampling Graphs and Data Table Tab 6 BHV -6 Air Sampling Graphs and Data Table Tab 7 BHV -7 Air Sampling Graphs and Data Table Tab 8 BHV -8 Air Sampling Graphs and Data Table C BHV Air Sampling Laboratory Results and QA/QC D Air Particulate Loading Graphs and Supporting Data E Environmental Gamma (OSL) Dosimeter Graphs and Supporting Data F Vegetation Graphs, Data Table, Laboratory Results and QA/QC G Stack Sample Laboratory Results H Surface Water Graphs and Field Data Sheets I Soil Sample Graphs, Data Table, Laboratory Results and QA/QC J Radon Monitoring Graphs and Data K Cell 2 Radon Flux Data ii WHITE MESA URANIUM MILL SEMI-ANNUAL EFFLUENT REPORT, JULY THROUGH DECEMBER 2016 1.0 INTRODUCTION The White Mesa Mill (the "Mill") has established monitoring programs to evaluate compliance with effluent limitations and to assess the potential for release of radioactive material into the local environment. These monitoring programs were developed and implemented at the time of Mill construction, operated with appropriate adaptation over time, and are consistent with the Mill's State of Utah Radioactive Materials License No. UT1900479 (the "License") and guidelines developed by the United States Nuclear Regulatory Commission ("NRC") (NRC Regulatory Guide 4.14, Radiological Effluent and Environmental Monitoring at Uranium Mills-Rev. 1, ML003739941), 1980). 1.1 Modifications to the Monitoring Programs As stated above, the monitoring programs implemented to date are consistent with the Mill's License and guidelines developed by the NRC and described in Regulatory Guide 4.14. The Mill's License was amended by the Division of Waste Management and Radiation Control ("DWMRC") on July 10, 2014. License Amendment 7 ("Amendment 7") dated July 10, 2014, among other things, modified and expanded the effluent monitoring programs implemented at the Mill. Amendment 7 required additional monitoring beyond what is regularly required by NRC Regulatory Guide 4.14. DWMRC requested the additional monitoring be documented in a revision to the Mill's Environmental Protection Manual ("EPM"). As required, EFRI submitted a revised EPM for DWMRC approval on September 8, 2014. A subsequent DWMRC Request for Information ("RFI") dated October 14, 2014 and e-mail correspondence dated October 20, 2014 added additional monitoring requirements beyond those specified in Amendment 7. EFRI incorporated the modifications resulting from the RFI and e-mail correspondence into an EPM revision submitted to DWMRC on November 18, 2014. The November 18, 2014 EPM was approved by DWMRC in a letter dated December 10, 2014. Specific changes to the individual monitoring programs resulting from Amendment 7, the RFI and the e-mail correspondence are discussed in the subsequent sections of this report. In addition, the EPM was updated in June and December 2016 to incorporate changes for equipment and correct typographical errors. In a letter dated July 23, 2014, DWMRC stated that because "Tailings Cell 2 is no longer in operation (receiving tailings), the Division of Air Quality and the Division of Radiation Control agree that Subpart W NESHAPs requirements ( 40 CFR Part 61) no longer apply; however, at this phase of cell 2 closure activities, the requirements of 10 CFR Part 40, Appendix A, Criterion 6 do apply." The July 23, 2014 letter further requires that radon flux measurements for Cell 2 be collected semi-annually in accordance with methodology specified in 40 CFR Part 61, Appendix B, Method 115 and that the measured results be included in the Semi-Annual Effluent Reports submitted to 1 DWMRC. As a result of the July 23 , 2014 letter, Cell 2 radon flux monitoring data are reported herein. Additional details regarding the monitoring and data collection activities for the Cell 2 radon flux are included in Section 9.0. As specified by the License and the documents described above, the Mill monitors the following environmental media and conditions: a) Airborne particulate radionuclide concentrations obtained from the following sampling stations: • North, east and south of the Mill Site: BHV-1, BHV-2, and BHV-8 (north), BHV-5 and BHV-7 (east), and BHV-4 (south). BHV-1 and BHV- 8 serve as surrogates for the nearest resident (BHV -1 and BHV -8 are approximately 1.2 miles north of the Mill, but approximately 0.4 miles closer to the Mill than the nearest resident); • A background location distant to and west of the Mill (BHV -3) that was monitored for airborne particulates up until November, 1995 (at which time background was established), which is no longer monitored for air particulates; and • A station specifically requested by the White Mesa Ute Community south of the Mill Site (BHV-6); b) External (direct) gamma radiation measured at air monitoring stations BHV-1, BHV-2, BHV-3, BHV-4, BHV-5, BHV-6, BHV-7, and BHV-8; c) Vegetation at three site periphery locations, for uptake of radionuclides; d) Stack release rates from the Mill's air emissions sources; e) Surface water at Cottonwood Creek and, when flowing, Westwater Creek, both located west of the Mill; f) Soil radionuclide activity during the third quarter of each year; g) Radon-222 at the air particulate monitoring stations (BHV -1 through BHV -8); h) Radon flux of the Cell 2 cover as specified by the DWMRC in correspondence dated July 23, 2014; i) Groundwater (up and down gradient) of the Mill facility; and1 j) Seeps and springs in the vicinity of the Mill. 1 1 Groundwater sampling and seeps and springs sampling are reported separately pursuant to the Mill's State of Utah Ground Water Discharge Permit No. UGW370004, and are not included with this report. 2 This semi-annual effluent report provides the results of the specific monitoring and sampling activities that were undertaken during the subject reporting period. 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING 2.1 Program Overview Prior to Amendment 7, the environmental airborne particulate monitoring program at the Mill utilized four air sampling stations. Four high-volume continuous air sampling stations (BHV-1, BHV-2, BHV-4, and BHV-5) were required by the License. In addition to these four environmental air sampling locations, an additional station (BHV -6) was installed at the request of the White Mesa Ute Community. This station began operation in July of 1999 and provides airborne particulate information in the southerly direction between the Mill and the White Mesa Ute Community. As stated in Section 1.1 above, Amendment 7 expanded the air particulate monitoring program. Amendment 7 included the following expansion of the air particulate monitoring program: • Addition of two air monitoring stations (BHV -7 and BHV -8); • Addition of thorium-232 ("Th-232") to the list of air particulate analytes; These sampling stations serve as sentinels for airborne particulate which could potentially emanate from the Mill site. In addition to its general site monitoring function, BHV -1 and BHV -8 also serve as conservative surrogates for concentrations at the nearest resident, because they are located approximately 1.2 miles north of the Mill just south of the nearest resident but between the Mill and that resident. With regard to background monitoring, the Mill previously operated a continuous high- volume air sampling station (BHV-3) which was located 3.5 miles west of the Mill site. With the approval of NRC, this station (BHV-3) was removed from the active air monitoring program in November 1995. At that time, NRC determined that a sufficient air monitoring database had been compiled at BHV -3 to establish a representative airborne radionuclide background for the Mill. The NRC approval to remove BHV -3 from the active air monitoring program specified background radionuclide concentrations based on the historic data. These concentrations are shown on the graphs and tables in Tab B3. While air sampling was discontinued at this location, gamma measurements and soil sampling continue at BHV-3. 2.2 Sampling Protocol and Analytical Results Airborne particulate monitors are operated continuously at each of the high-volume air sampling stations except BHV-3. As noted above, BHV-3 was removed from the active 3 air monitoring program in November 1995, but the NRC specified background concentrations are shown in Attachment B. Particulate sample collection filters are gathered by site technicians weekly in accordance with the Mill's environmental air sampling procedures and are composited on a quarterly basis for laboratory analyses. The collected filters are analyzed for Unat activity, Th-230 activity, Ra-226 activity, Th-232 activity and Pb-210 activity. Fugitive dust standards for the facility are limited by the Mill's State of Utah Air Approval Order. The specific locations of the Mill's airborne particulate monitoring stations are depicted on the figure entitled Particulate Monitoring Stations included as Attachment A. Station BHV-3, which is no longer sampled for air particulates, is located approximately 3.5 miles west of the Mill facility and is not shown on the Figure. The analytical results of radionuclide particulate sampling for each monitoring station operated during this reporting period are provided in Attachment B under separate sampling station attachment tabs (Tabs 1-8). Each tab contains graphical illustrations of the radionuclide concentrations in log-scale presentation format. The graphs display reported data over time since the 1981 inception of the Mill's environmental air particulate monitoring program or the installation of the locations, whichever is appropriate. The actual analytical results (and associated QNQC information) reported by the laboratory for the reporting period are provided under Attachment C. In addition to the analyses for radionuclides, particulate loading is determined for each filter and composited as a quarterly mass-loading estimate for review purposes only. Graphs showing particulate loading at each station and the underlying data are included as Attachment D. Analytical data were reviewed against the laboratory established acceptance limits specified in the data packages. The analytical data are usable for their intended purpose. Any deviations noted did not affect the quality or usability of the data. For graphical illu tration purpo es values reported at zero, value reported at le s than the ~rescribed detection limit(< 1 x 10'16 uCi/mJ), and mj ·sjng value were plotted as 1 x 10·1 uCi/ml concentrations. Where other "le than' values were indicated {i.e. where detection limits for the data varied from 1 X 10'16 uCi/ml), the detection limit concentration was utilized for plotting the data point. This graphing convention is not utilized to formulate station average information, nor is it intended as a precedent for data treatment. Rather, the intent is to provide a conservative viewable depiction of site airborne radionuclide information. This is considered to be a conservative approach, because the actual concentration below the detection limit cannot be determined and, as a result, the plotted point will be at the same or a higher concentration than the actual activity concentration of the collected sample. 4 2.3 General Observations The results of environmental air monitoring for this semi-annual period indicate that for all radionuclides at all monitoring stations, airborne radionuclide particulate activity concentrations were well below regulatory Effluent Concentration Limits ("ECL's") and the Mill's ALARA goals, which are set at 25% of the ECLs, except as noted below. It is noteworthy and expected that Pb-210 concentrations are elevated when compared to the other parent radionuclide concentrations (i.e. U-nat, Th-230 and Ra-226). This phenomenon is due to the well-established controlling effect experienced worldwide as a result of the ubiquitous presence of radon in the earth's atmosphere. Accordingly, the elevated Pb-210 presence in disequilibrium with parent radionuclides measured here is not associated with uranium milling operations. Rn-222 emanates as a decay-chain progeny of the Ra-226 contained in the soil of the earth's crust and is dispersed generally throughout the earth's atmosphere. The electrically charged short and long-lived decay products of Rn-222 attach to ambient dust particles found naturally in the atmosphere and are carried with the air. Pb-210 is the longest lived of these decay products and is the decay product of the shorter-lived radon progeny. As such, it accumulates as an electrical attachment on the natural ambient dust in the atmosphere and is generally measured at elevated activity when compared to local decay-chain parent radionuclide activity, regardless of uranium milling activity. At the Mill's BHV air monitoring stations, all dust (ambient natural and mill derived) is collected by the sample filter. Because of the natural elevation of Pb-210 accumulated as an attachment to the naturally occurring ambient dust particles collected by the air sampling equipment, Pb-210 is commonly elevated and in disequilibrium when compared to parent radionuclide activity, regardless of the Mill's presence. By way of illustration, average ground-level concentrations have been reported for selected States (NCRP Report 94, 1992) and are summarized in Table 1 in the Tables Tab of this report, demonstrating that elevated Pb-210 activity is present where no uranium milling operations are located nearby. In April 1977, prior to Mill construction and Mill operation , air particulate Pb-210 was measured at the Mill site to be 1.3E-14 uCi/rnl (13 .0E-3 pCi/m3/. 2.4 Site Specific Sampling Data The results of airborne particulate monitoring for the period (without background subtraction) are provided by sampling station and radionuclide in Tables 2 through 6 in the Tables Tab of this report. Along with these data, the tables present comparative ECL' s and the ECL percentage measured at each of the monitoring stations sampled during the period. A review of these data support the conclusion that airborne particulates are well controlled at the Mill. In all cases, the measured activity concentrations were well within the ECL, as well as the Mill's ALARA goal (i.e. 25% of the ECL). Lower 2 See the Environmental Report, White Mesa Uranium Project, San Juan County, Utah for Energy Fuels Nuclear, Inc. prepared by Dames & Moore, January 30, 1978, Section 2.9.1.1 5 Limits of Detection consistent with NRC Regulatory Guide 4.14 were maintained by the Mill's contract analytical laboratory for this reporting period. The data obtained since program inception in 1981 indicates that only one individual quarterly measurement (Th-230 at BHV-5 for the 2nd Quarter of 1996) has ever exceeded the ECL at the Mill. While it is important to consider and evaluate an individual measurement exceeding the ECL, it is the average annual concentration that is of primary significance for public dose estimation purposes. In that instance, the average annual concentration of Th-230 for BHV-5 in 1996 was well below the ECL. Data obtained since program inception in 1981 also indicate that, with very few exceptions, the gross (background inclusive) measurements do not exceed the site's ALARA goal (i.e. only ten of the several thousand total gross radionuclide determinations to date exceeded the Mill's self-imposed 25% ALARA goal). 2.5 Radon-222 With the approval of the NRC, Radon-222 monitoring at BHV stations at the Mill was discontinued in 1995 due to the unavailability of monitoring equipment to detect the revised 10 CFR Part 20 standard. Instead, compliance with these limits and the requirements of R313-15-301 was demonstrated by a calculation, authorized by the NRC and as contemplated by R313-15-302(2)( a) which states "A licensee or registrant shall show compliance with the annual dose limit in Section R313-15-301 by: (a) Demonstrating by measurement or calculation that the total effective dose equivalent to the individual likely to receive the highest dose from the licensed or registered operation does not exceed the annual dose limit;". This calculation is performed by use of the MILDOS code for estimating environmental radiation doses for uranium recovery operations. R313-15-302(2)(a) contemplates demonstrating compliance either through modeling or measurement. In order to determine whether or not detection equipment has improved since 1995, EFRI voluntarily began ambient Radon-222 monitoring at the BHV stations in 2013. The Radon-222 data collected from 2013 through present are presented in Attachment J. As stated in Section 1.1 above, Amendment 7 expanded the Mill's effluent monitoring programs in 2014. Amendment 7 included expanding the monitoring programs to require the collection of Radon-222 data at all of the BHV stations. For the BHV stations EFRI calculated ECLs using methodology shown in Attachment J. The calculated ECLs for all of the BHV stations are included on the data table included in Attachment J. The radon- 222 results are below the calculated ECLs and within the range of historic levels as shown in Attachment J. Radon-222 monitoring is completed using detectors with an effective reporting limit of 0.06 pCi/L. Field blank detectors are collected quarterly and the results (with background included) are included in Attachment J. 6 During the reporting period, one field blank was collected during each quarter. Field blanks are opened at the beginning of the monitoring period and immediately sealed with the manufacturer supplied foil seals. The field blanks are stored in a sealed foil pouch in the environmental· office until the end of the monitoring period, when they are packaged with the field samples and shipped to the laboratory for processing. While relatively low concentrations were reported for the field blanks, the field blank data show detections which are greater than the highest detection reported for any of the samples collected at the high volume stations. The field blank data have been consistently higher than the samples. Despite the detections reported for the field blanks, there is no indication that the results reflect contamination during shipping. If the detections on the field blanks indicated contamination resulting from shipment, then all of the detectors would be affected in the same manner and the sample data are below the field blank levels. It appears that the field blanks have been affected by the storage prior to shipping. EFRI is conducting an investigation into the possible causes of the anomalous field blank detections. 3.0 EXTERNAL RADIATION (DIRECT GAMMA) Gamma exposure rate estimates were measured for the reporting period utilizing optically stimulated luminescence dosimeters ("OSLs"). Previously, these dosimeters were located at each of the Mill's high-volume air sampling stations (BHV-1, BHV-2, BHV-4, BHV-5 and BHV-6) and at the designated background monitoring station (BHV-3). As noted in Section 1.1 of this report, Amendment 7 expanded the effluent monitoring programs at the Mill. Amendment 7 included expansion of the gamma exposure monitoring program through the addition of gamma monitoring at the two new air monitoring stations (BHV-7 and BHV-8). Measurements obtained from location BHV -3 have been designated as background due to BHV-3's remoteness from the Mill site (i.e., BHV-3 is located approximately 3.5 miles west of the Mill site). The results of the environmental OSL measurements and semi- annual cumulative above-background data are provided in Table 7 in the Tables Tab of this report. In addition, measurement data obtained at these locations are graphically presented in Attachment E to this report. The results for this period indicate that above background measurements for stations BHV-1, BHV-2, BHV-4, BHV-5, BHV-6, BHV-7, and BHV-8 are within regulatory limits. BHV-1 and BHV-8 are at the location of the nearest potential residence. The nearest actual residence is approximately 0.4 miles north of BHV -1 and BHV -8. The annual limit for an individual member of the public is 100 mrem/yr for combined internal and external exposure. 4.0 VEGETATION SAMPLES Vegetation samples are collected at three locations around the Mill property. The sampling locations are: 1) northeast, 2) northwest and 3) southwest of the Mill facility. 7 The NRC Regulatory Guide 4.14 requires that three samples be collected during the grazing season, without specifying exact months or times during the season. As noted in Section 1.1, Amendment 7 and the associated RFI expanded the vegetation sampling program through the addition ofTh-232 and U-Nat. During the July through December reporting period, samples were collected on November 11, 2016. The data from the November 2016 sampling event are included in the in Attachment F. Graphical log-scale presentation of the vegetation sampling results, together with the analytical results reported by the Mill's contract laboratory (including QA/QC information) for this sampling period, are included as Attachment F of this report. The 2016 data results are within the variation of previous sampling episodes. Analytical data were reviewed against the laboratory established acceptance limits specified in the data packages. The analytical data are usable for their intended purpose. Any deviations noted did not affect the quality or usability of the data. The value in the MDC column in the data package is the sample-specific minimum detectable concentration ("MDC"). The MDC is based on the sample moisture, composition and other sample-specific variables. The lower limit of detection which is a limit representing the detection capability of the measurement system is referred to as the Reporting limit ("RL") in the data package. 5.0 STACKSAMPLING Under Section 5.0 of Tab 1.4 of the Mill's Environmental Protection Manual, Revision: EFR-4, 11114 (the "Environmental Protection Manual") as modified in response to DWMRC e-mail correspondence dated October 20, 2014, gas stack samples are collected at the Mill in accordance with the schedule shown below: Stack Sampling Requirements Grizzly North and/or Yellowcake Vanadium South Packaging Vanadium Frequency Baghouse Yellowcake Baghouse Dryer Stack Packaging Stack Dryer Stacks Stack Stack Quarterly If operating, If operating, If operating, If operating, If operating, U-nat, Th-U-nat, Th- U-nat, Th-U-nat, Th-U-nat, Th- 230, Ra-226, 230, Ra-226, 230, Ra-226, 230, Ra-226, 230, Ra-226, Pb-210, Th-Pb-210, Th-Pb-210, Th-Pb-210, Th-Pb-210, Th- 232, Ra-228, 232, Ra-228, 232, Ra-228, 232, Ra-228, 232, Ra-228, and Th-228. and Th-228. and Th-228. and Th-228. and Th-228. 8 The analytical results of stack sampling conducted in the reporting period, as well as for the previous two quarters, are provided in Table 8 in the Tables Tab of this report. The actual analytical results reported by the laboratory for the reporting period (third and fourth quarters 20 16) are provided in Attachment G to this report. The south yellowcake dryer and yellowcake baghouse operated during the third and fourth quarters of 2016. The grizzly operated during the third quarter 2016. The north yellowcake dryer has not been in operation since the third quarter of 2012, and therefore, has not been sampled since it was last in operation. The vanadium dryer and vanadium packaging stack did not operate during the reporting period and were not sampled. It is also important to note that stack effluent concentrations are not comparable to environmental air sampling station ECLs for regulatory compliance purposes. The ECL is a limit that applies to the receptor locations and is not applicable to effluents from mill processes on the Mill site. These stack release data are more appropriately utilized for dose modeling purposes, and dose modeling is not computed for semi-annual reporting purposes. Analytical data were reviewed against the laboratory established acceptance limits specified in the data packages. The analytical data are usable for their intended purpose. Any deviations noted did not affect the quality or usability of the data. 6.0 SURFACE WATER MONITORING Under the License, Part 11.2 B surface water samples are required to be obtained annually from Westwater Canyon and semi-annually from Cottonwood Creek. Sediment samples from Westwater Canyon are taken in place of the Westwater Canyon surface water sample where surface water is not available for sampling. Westwater Canyon surface water was not sampled in 2016, because no water was present during this reporting period. A sediment sample was collected in August 2016. Attempts to collect a surface water sample from Westwater Canyon continued throughout the third and fourth quarters of 2016 but were unsuccessful. Documentation of the attempted sample collection is included in Tab H for the third and fourth quarters of 2016 and in the previous Semi-Annual Effluent Report for the first and second quarters of 2016. The Mill's Environmental Protection Manual requires that samples from Cottonwood Creek be analyzed for TDS and total suspended solids ("TSS") quarterly, and the License, Part 11.2 B requires that samples from Cottonwood Creek be analyzed for dissolved and suspended radionuclides including Gross Alpha, U-nat, Ra-226, and Th- 230 semi-annually. Cottonwood Creek surface water was not sampled in the third or fourth quarters of 2016, because no water was present during this reporting period. Documentation of the attempted sample collection is included in Tab H. The field data sheets for the attempted surface water sampling events, along with graphs showing historic results are included as Attachment H. The results of the historic 9 sampling indicate that surface water concentrations remain low and within the range of a typical surface water. 7.0 SOIL SAMPLING As mentioned in Section 1.1 above, specific changes to the individual monitoring programs have been made as a result of Amendment 7, the RFI, and e-mail correspondence with DWMRC. In accordance with the Mill's EPM, surface soils were collected in August 2016. The soil samples were analyzed, on a dry basis, for Ra-226, U-nat, Pb-210, and Th-232. The results of these samplings indicate that soil activity levels at the air monitoring stations remain low and within the range of historic levels. A graphical presentation of the soil results, together with analytical sample results for the August 2016 sampling event are provided in Attachment I. Analytical data were reviewed against the laboratory established acceptance limits specified in the data packages. The analytical data are usable for their intended purpose. Any deviations noted did not affect the quality or usability of the data. Field duplicate sample results were assessed as required by the SOP. Duplicate results were within the acceptance limits specified in the SOP except as noted in Table 1-3. The approved SOP specifies a separate corrective action for duplicate RPDs outside of acceptance limits. The revised procedure for duplicate results outside of acceptance limits was implemented for the results outside of the acceptance limits. The corrective actions that were taken in accordance with the SOP procedure are as follows: the QA Manager contacted the Analytical Laboratory and requested a review of the raw data to assure that there were no transcription errors and the data were accurately reported. The laboratory noted that the data were accurate and reported correctly. Reanalysis was not completed as the samples were disposed of by the laboratory. Field duplicate results are shown in Attachment I. 8.0 METEOROLOGICAL MONITORING As in prior reporting periods, an independent contractor has prepared the White Mesa Mill Semi-annual Meteorological Monitoring Report for the period of July through December 2016. This information is retained at the Mill site for agency review. 9.0 CELL 2 RADON FLUX The July 23, 2014 letter, DWMRC stated that because "Tailings Cell 2 is no longer in operation (receiving tailings), the Division of Air Quality and the Division of Radiation Control agree that Subpart W NESHAPs requirements (40 CFR Part 61) no longer apply; however, at this phase of cell 2 closure activities, the requirements of 10 CFR Part 40, Appendix A, Criterion 6 do apply." 10 Further, the DWMRC July 23, 2014 letter states that "since the Mll-DOS-Area Models that have been run to show compliance with dose limits for releases from the Mill were based on a limit of 20 picocuries per square meter second (pCi/m2-sec), in order to ensure compliance with previously analyzed conditions, the DWMRC will require the licensee to continue to measure the radon flux in accordance with 40 CFR 61, Appendix B, Method 115, "Monitoring for Radon-222 Emissions" (2013). The measured radon flux for Cell 2 shall not exceed a value of 20 (pCilm2-sec) until a new Mll..-DOS-Area Model to analyze a higher radon flux is completed and demonstrates compliance with dose limits based on the releases from the Mill. As required by Method 115, a minimum of 100 measurements are required and shall be performed on a semi-annual basis." Per the requirements detailed above, EFRI sampled Cell 2 radon flux in July 2016 for the July through December 2016 reporting period. The July 2016 measurement was 7.0 pCi/(m2-sec). The July measurement was below the 20.0 pCi/(m2-sec) standard. The full data report for the July 2016 Cell 2 radon flux sampling is provided in Attachment K. It is important to note that Cell 2 Phase 1 cover placement/construction commenced in April 2016 and continued throughout 2016. The Phase 1 cover activities include the placement and compaction of approximately 4.5 feet of soil materials. 11 10.0 SIGNATURE AND CERTIFICATION This document was prepared by Energy Fuels Resources (USA) Inc. on February 27, 2017. ENERGY FUELS RESOURCES (USA) INC. By: Scott A. Bakken Senior Director Regulatory Affairs 12 Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Scott A. Bakken Senior Director Regulatory Affairs Energy Fuels Resources (USA) Inc. 13 TABLES Table 1-NCRP Report 94-Global Pb-210 Concentration Example State Pb-210 Concentratien liBq/M3 11Ci/~l California 600 1.60E-14 Illinois 1500 4.10E-14 Ohio 300 8.10E-15 Massachusetts 700 1.90E-14 Table 2-Air Monitoring Station Results U-Nat (Comparison to Limits) 3rd and 4th Quarter 2016 Monitoring 3rd 4th Effluent Average Station Qtr.Result Qtr.Result Concentration PercentECL (uCi/ml) (uCi/ml) Limit (ECL) (uCI/ml) BHVl l.lOE-15 9.80E-16 9.00E-14 1.16E+00 BHV2 4.20E-16 4.10E-16 9.00E-14 4.61E-Ol BHV4 6.20E-15 4.10E-15 9.00E-14 5.72E+00 BHV5 ?.IOE-15 5.10E-15 9.00E-14 6.78E+00 BHV6 6.90E-15 8.90E-15 9.00E-14 8.78E+00 BHV7 2.60E-15 1.60E-15 9.00E-14 2.33E+00 BHV8 1.20E-15 1.20E-15 9.00E-14 1.33E+00 Table 3 -Air Monitoring Station Results Th-230 (Comparison to Limits) 3rd and 4th Quarter 2016 Monitoring 3rd 4th Effluent Average Station Qtr.Result Qtr.Result Concentration Percent ECL (uCi/ml) (uCi/ml) Limit (ECL) (uCI/ml) BHVl 8.70E-17 7.80E-17 2.00E-14 4.13E-Ol BHV2 6.90E-17 1.90E-17 2.00E-14 2.20E-Ol BHV4 4.40E-16 3.00E-16 2.00E-14 1.85E+00 BHV5 7.60E-16 6.60E-l6 2.00E-14 3.55E+00 BHV6 4.00E-16 3.30E-16 2.00E-14 1.83E+00 BHV7 l.?OE-16 1.20E-16 2.00E-l4 7.25E-Ol BHV8 8.40E-17 6.00E-17 2.00E-14 3.60E-Ol Table 4-Air Monitoring Station Results Ra-226 (Comparison to Limits) 3rd and 4th Quarter 2016 Monitoring 3rd 4th Effluent Average Station Qtr.Result Qtr.Result Concentration Percent ECL (uCi/ml) (uCilml) Limit (ECL) (uCI/ml) BHVl 1.80E-16 l.30E-16 9.00E-13 l.72E-02 BHV2 8.10E-l7 5.00E-17 9.00E-13 7.28E-03 BHV4 2.20E-15 4.80E-16 9.00E-13 1.49E-Ol BHV5 l.IOE-15 9.60E-16 9.00E-13 1.14E-Ol BHV6 7.20E-16 4.80E-16 9.00E-13 6.67E-02 BHV7 4.10E-16 2.50E-16 9.00E-13 3.67E-02 BHV8 3.30E-16 8.50E-l7 9.00E-l3 2.31E-02 Table 5 -Air Monitoring Station Results Pb-210 (Comparison to Limits) 3rd and 4th Quarter 2016 Monitoring 3rd 4th Effluent Average Station Qtr.Result Qtr.Result Concentration Percent ECL (uCilml) (uCilml) Limit (ECL) (uCI/ml) BHVl 1.20E-14 2.20E-14 6.00E-13 2.83E+00 BHV2 l.OOE-14 2.IOE-14 6.00E-13 2.58E+00 BHV4 3.40E-16 2.20E-14 6.00E-13 1.86E+00 BHV5 2.90E-16 2.10E-14 6.00E-13 1.77E+00 BHV6 3.20E-15 2.10E-14 6.00E-13 2.02E+00 BHV7 2.80E-15 l.SOE-14 6.00E-13 1.48E+00 BHV8 7.60E-15 1.40E-14 6.00E-13 1.80E+00 Table 6 -Air Monitoring Station Results Th-232 (Comparison to Limits) 3rd and 4th Quarter 2016 Monitoring 3rd 4th Effluent Average Station Qtr.Result Qtr.Result Concentration PercentECL (uCi/ml) (uCi/ml) Limit (ECL) (uCI/ml) BHVl 9.50E-18 4.80E-18 4.00E-15 1.79E-Ol BHV2 5.20E-17 2.20E-18 4.00E-15 6.78E-01 BHV4 7.10E-18 4.50E-18 4.00E-15 1.45E-Ol BHV5 3.00E-17 1.30E-17 4.00E-15 5.38E-01 BHV6 1.20E-17 9.50E-18 4.00E-15 2.69E-Ol BHV7 5.50E-18 4.80E-18 4.00E-15 1.29E-Ol BHV8 4.70E-18 3.20E-18 4.00E-15 9.88E-02 Table 7 -Environmental Optically Stimulated Luminescence Dosimeter Measurements (Gamma) ~Nl 4!fh' 3rd Quarter 4th Quarter Cumulative ¢!1I<a11"00F Q~ter Result Less Result Less Semiannual Mont:t.0I"ing B~mft De llll't Background Background Estimate s~~ltti<if.a {il;urenil) .CJ1u,el~ (mrem) (mrem) (mrem) BHV1 46.6 38.2 5 4 9 BHV2 43.4 39 1.8 4.8 6.6 BHV3 41.6 34.2 0 0 0 BHV4 40.9 35.4 0 1.2 1.2 BHV5 40 36.3 0 2.1 2.1 BHV6 39.9 34.6 0 0.4 0.4 BHV7 39.5 38.5 0 4.3 4.3 BHV8 42.4 36 0.8 1.8 2.6 l.$t\,ltr.'~10 No stack sampli.ng was conducted as the dryers did not run. No grimling or packaging was completed during the 1st quarter. -· ·2nd'Qtr. 2{}16 U-Nat U-Nat. Th-228 Th-228 Th-230 Th-230 Th-232 Th-232 Pb-210 Pb-210 Ra-226 Ra-226 Ra-228 Ra-228 uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec SYC Dryer Scrubber I 1.05E-09 1.20E-04 1.09E-14 1.24E-09 2.56E-14 2.92E-09 1.50E-I 5 1.72E-JO 8.24E-J 3 9.41 E-08 1.58E-14 I .80E-09 4.67E-13 5.34E-08 SYC Dryer Scrubber 2 I .02E-09 1.13E-04 2.89E-15 3.19E-IO 2.30E-14 2.54E-09 5.95E-16 6.55E-l I 1.15E-12 1.26E-07 2.59E-14 2.85E-09 8.14E-13 8.97E-08 YC Packaging Baghouse 4.72E-10 1.18E-05 2.67E-15 6.69E-1 I 6.53E-14 1.64E-09 1.14E-15 2.85E-J I 1.55E-13 3.89E-09 3.42E-14 8.56E-IO 2.70E-12 6.77E-08 3rd,Qtr. 2016 U-Nat U-Nat. Th-228 Th-228 Th-230 Th-230 Th-232 Th-232 Pb-210 Pb-210 Ra-226 Ra-226 Ra-228 Ra-228 uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec SYCDryer Scrubber 1 3.01E-JO 3.69E-05 2.46E-15 3.02E-10 2.57E-14 3.15E-09 1.49E-15 1.83E-IO 7.25E-13 8.91E-08 2.53E-14 3.!0E-09 3.76E-13 4.62E-08 SYCDryer Scrubber 2 5.57E-IO 6.69E-05 4.49E-15 5.39E-10 4.71E-13 5.65E-08 1.28E-14 1.54E-09 1.97E-12 2.37E-07 7.78E-13 9.34E-08 3.41E-13 4.09E-08 YC Packaging Baghouse 4.04E-09 1.46E-04 1.95E-14 7.09E-IO l.IOE-13 4.00E-09 S.IOE-15 1.85E-10 8.65E-12 3.14E-07 1.32E-13 4.79E-09 2.1 lE-12 7.66E-08 I Grizzly 2.37E-Jl 3.44E-06 8.94E-I6 l.30E-10 3.01E-13 4.39E-08 3.38E-15 4.92E-IO 3.86E-13 5.62E-08 4.66E-13 6.79E-08 2.34E-13 3.40E-08 4th Qtr. 2016 I U-Nat U-Nat. Th-228 Th-228 Th-230 Th-230 Th-232 Th-232 Pb-210 Pb-210 Ra-226 Ra-226 Ra-228 Ra-228 uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec SYCDryer I Scrubber I 9.30E-10 8.76E-05 3.54E-14 3.34E-09 1.77E-14 1.67E-09 O.OOE+OO O.OOE+OO l.26E-12 1.18E-07 2.53E-12 2.39E-07 2.13E-13 2.00E-08 I SYC Dryer I Scrubber 2 4.28E-JO 3.95E-05 3.61E-14 3.34E-09 l.80E-14 1.67E-09 5.41E-15 5.00E-JO 1.71E-12 1.58E-07 3.26E-12 3.02E-07 2.16E-13 2.00E-08 YL 1'3CKagmg Baghouse J.67E-I I 5.25E-07 2.12E-14 6.67E-l0 5.29E-14 1.67E-09 2.12E-14 6.67E-l0 1.43E-12 4.50E-08 8.89E-12 2.80E-07 6.35E-13 2.00E-08 ATTACHMENT A HIGH VOLUME AIR MONITORING STATIONS Legend + Air Monitoring Station c:::J Township and Range ~~ n Property Boundary c=J Section c:::J Tailings Cell L_ l Pond --Road ----~ Canyon Rim Drainage Coordinate System: NAD 1983 StatePiane Utah South FIPS 4303 Feet Date: WHITE MESA MILL By: County: San Juan State: Utah Location:. ATTACHMENT A PARTICULATE MONITORING STATIONS Author: rellis Date: 2/20/2017 Drafted By: rellis Energy Fuels Resources Inc. White Mesa Mill High Volume Air Monitoring Stations Coordinates Air Station Northing Easting Ground Elevation* BHV-1 10171106.23 2222420.22 5678.37 BHV-2 10180701.63 2223565.12 5789.20 BHV-4 10159480.63 2216380.00 5544.79 BHV-5 10164004.22 2221859.34 5590.50 BHV-6 10160451.77 2221996.62 5578.61 BHV-7 10170920.58 2219311.48 5660.72 BHV-8 10167873.94 2222236.08 5634.74 Coordinate System: Modified Utah State Plane-NAD83-South Zone-US Survey Feet *Using Fisher Survey Vertical Datum ATTACHMENT B BHV AIR SAMPLING GRAPHS AND DATA TABLES TAB 1 BHV-1 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent 9E-14 uCi/ml 8HV-1U Effluent ZE-14 uCi/ml BHV-1TZ30 Effluent 9E-13 uCi/ml BHV-1R Effluent 6E-13 uCi/ml BHV-1PB Effluent 4e-15 uCi/ml BHV-1TZ32 Concentration Concentration Concentration Concentration concentration Limit= limit= Umit= Limit= Umit= ~ .. ALARAGoal= 2.25E-14 uCi/ml ALARA Goal= SE-15 uCi/ml ALARAGoal= 2.25E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml ALARAGoal = lE-15 uCi/ml Pre 1994MPC SE-UuCi/ml Pre 1994 MPC SE-14 uCi/ml Pre 1994 MPC ZE-12 uCi/ml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable j.imlt= Limit= Limit= Limit= Limit= Pre 1994 l.ZSE-12 uCi/ml Pre 1994 SE-13 uCi/ml Pre 1994 lE-12 uCi/ml Pre 1994 Not Applicable ALARAGOAL= ALARAGOAL= ALARAGOAL= ALARAGOAL= Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 2.35E·15 S.OOE-12 1.25E-12 7.82E-16 8.00E-14 2.00E-14 1.06E-15 2.00E-12 S.OOE-13 2.57E-14 4.00E·12 l.OOE-12 Not Anajyzed Not Applicable Not ApJ:>Iicable - 12/14/1981 1.56E-15 5.00E-12 1.25E-12 1.49E-15 8.00E-14 2.00E-14 1.93E-15 2.00E-12 S.OOE-13 2.64E-14 4.00E-12 l.OOE-12 Not AnaJyzed Not Applicable Not Applicable 3/29/1982 2.16E-15 S.OOE-12 1.25E-12 2.93E-15 8.00E-14 2.00E-14 1.16E-15 Z.OOE-12 S.OOE-13 2.09E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 6/30/1982 4.69E-15 5.00E-12 l.25E-12 3.46E-15 8.00E-14 2.00E-14 2.38E·15 2.00E-12 5.00E-13 2.14E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 9/27/1982 4.45E·15 's.OOE-12 1.25E-12 3.29E-15 B.OOE-14 2.00E-14 3.23E-15 Z.OOE-12 5.00E-13 1.99E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 1/3/1983 4.39E-15 5.00E-12 1.25E-12 5.91E-16 B.OOE-14 2.00E-14 9.14E-16 Z.OOE-12 5.00E-13 4.87E-14 4.00E-12 l.OOE-12 Not Analyzed Jllot Ai>plicable Not Applicable 4/4/1983 7.51E-16 S.OOE-12 1.25E-12 2.13E-16 S.OOE-14 2.00E-14 3.20E-16 2.00E-12 s.OOE-13 1.88E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable • Not Applicable 6/30/1983 2.68E-16 S.OOE-12 1.25E-12 6.92E-16 S.OOE-14 2.00E·14 7.92E-16 Z.OOE-12 5.00E-13 2.00E-14 4.00E·12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 10/3/1983 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 s.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 1/3/1984 2.87E-15 S.OOE-12 1.25E-12 1.14E-16 8,00E-14 2.00E-14 1.79E-16 2.00E-12 5.00E-13 1.06E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 4/2/1984 1.59E-15 S.OOE-12 1.25E-12 3.40E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 S,OOE-13 3.34E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable . Not ~plicable 7/2/1984 3.10E-15 S.OOE-12 1.25E-12 l.OOE-15 8.00E-14 2.00E-14 2.09E-15 2.00E-12 s.OOE-13 1.88E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 10/1/1984 6.42E-16 5.00E-12 1.25E-12 1.39E-16 8.00E-14 2.00E-14 1.94E-16 2.00E-12 S.OOE-13 1.85E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 1/2/1985 5.06E-16 S.OOE-12 1.25E-12 4.56E-16 B.OOE-14 2.00E-14 3.49E-16 2.00E-12 5.00E-13 3.03E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 4/1/1985 O.OOE+OO S.OOE-12 1.25E·12· 1.23E-15 S.OOE-14 2.00E-14 4.88E-16 2.00E-12 5.00E-13 8.06E-15 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 7/1/1985 7.17E-16 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 1.05E-15 2.00E-12 5.00E-13 2.15E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 9/30/1985 6.13E-~6 S.OOE-12 1.25E-12 1.18E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 5.00E-13 3.64E-15 4.00E·12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 1/2/1986 3.42E-15 S.OOE-12 1.25E-12 4.74E-16 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 4/1/1986 3.98E·15 5.00E-12 -1.25E-12 9.74E-16 B.OOE-14 2.00E-14 1.50E-15 2.00E-12 S.OOE-13 1.41E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 6/30/1986 $.51E-17 5.00E-12 1.25E-12 3.52E-16 8.00E·14 2.00E-14 1.37E-15 2.00E-12 S.OOE-13 1.23E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 10/27/1986 1.99E-15 5.00E-12 1.25E-12 3.06E-16 8.00E-14 2.00E-14 1.25E-15 2.00E-12 s.OOE-13 1.08E-14 4.00E-12 1.00E·12 Not Analyzed Not Applicable Not Applicable 12/15/1986 l.67E-15 S.OOE-12 1.25E-12 1.16E-16 8.00E-14 2.00E-14 5.98E-16 2.00E-12 S.OOE-13 1.37E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 3/16/1987 2.33E-15 S.OOE-12 1.25E-12 4.30E-16 8.00E-14 2.00E-14 1.92E-16 2.00E-12 S.OOE-13 5.59E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 5/11/1987 2.36E·15 5.00E-12 "1.25E-12 7.69E-16 8.00E-14 2.00E-14 8.76E-16 2.00E-12 S.OOE-13 1.45E-14 4,00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 9/9/1987 2.27E-15 5.00E-12 1.25E-12 2.44E-15 8.00E-14 2.00E-14 8.51E-16 2.00E-12 S.OOE-13 3.14E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/2/1987 2.75E-15 5.00E-12 1.25E-12 1.46E-15 8.00E-14 2.00E-14 1.34E-15 2.00E-12 S.OOE-13 2.79E-14 4.00E-12 l.OOE-12 NOt Analyzed Not Applicable Not Applicable 2/16/1988 1.07E-15 5.00E-12 l.25E-12 1.47E-16 8.00E-14 2.00E-14 4.44E-16 7.00E-12 S.OOE-13 4.01E-14 4.00E·12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/18/1988 1.98E-15 5.00E-12 1.25E-12 1.25E-15 8.00E-14 2.00E-14 6.40E-16 2.00E-12 5.00E-13 1.07E-14 4.00E-12 l.OOE-12 NOt Analyzed Not Applicable Not Applicable 8/15/1988 ~.06E-15 5.00E-12 1.25E-12 3.41E-15 B.OOE-14 2.00E-14 5.08E-16 2.00E-12 5.00E-13 1.62E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/14/1988 3.94E-15 5.00E-12 1.25E-12 2.12E-15 8,00E-14 2.00E-14 1.01E-15 ?.OOE-12 5.00E-13 2.47E-14 4.00E-12 1,00E-12 Not Analyzed Not Applicable Not Applicable 2/13/1989 1.99E-15 5.00E-12 1.25E-12 5.73E-16 8.00E-14 2.00E-14 5.99E-16 2.00E-12 5.00E-13 3.23E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable I 5/15/1989 1.70E-15 5.00E-12 1.25E-12 6.32E-16 8.00E-14 2.00E-14 5.86E-16 2.00E-12 S.OOE-13 6.16E-15 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable ! 8/14/1989 2.31E-15 5.00E-12 1.25E-12 2.31E-16 8,00E-14 2.00E-14 1.77E-16 l.OOE-12 5.00E-13 7.65E-15 4.00E-12 1.00E-12 NOt Analyzed Not Applicable Not Applicable i 11/13/1989 4.72E-15 S.OOE-12 1.25E-12 1.71E-15 8.00E-14 2.00E-14 1.52E-15 2.00E-12 S.OOE-13 1.89E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable I 2/12/1990 3.44E-16 S.OOE-12 1.25E-12 8.39E-16 8.00E-14 2.00E-14 8.31E·l6 'Z.OOE-12 S.OOE-13 2.57E-14 4.00E-12 1,00E-12 Not Analyzed Not Applicable Not Applicable I 5/14/1990 3.03E-15 5.00E-12 1.25E-12 1.47E-15 8.00E-14 2.00E-14 1.04E-15 l.OOE-12 5.00E-13 1.79E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not ARplicable I 8/13/1990 1.64E-15 5.00E-12 1.25E-12 1.49E-15 8.00E-14 2,00E-14 3.34E-16 l.OOE-12 S.OOE-13 8.27E-15 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable I I 11/12/1990 1.48E-15 5.00E-12 1.25E-12 7.50E-16 8.00E-14 2.00E-14 5.80E-16 2.00E-12 5.00E-13 2.16E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable I 2/11/1991 1.90E·16 5.00E-12 1.25E-12 3.48E-17 8.00E-14 2.00E-14 7.91E-17 2.00E-12 S.OOE-13 3.79E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable I 5/13/1991 '3.42E-16 s.OOE-12 1.25E-12 1.34E-15 B.OOE-14 2.00E-14 7.39E-16 2.00E-12 S.OOE-13 1.46E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable I 8/12/1991 2.77E-16 S.OOE-12 1.25E-12 4.17E-17 8.00E-14 2.00E-14 1.45E-16 l.OOE-12 5.00E-13 1.80E-14 4.00E-12 1.00E·12 Not Analyzed Not Applicable Not Applicable I 11/11/1991 _6.65E-17 S.OOE-12 1.25E-12 9.13E-17 8.00E-14 2.00E-14 2.77E-17 2.00E-12 5.00E-13 1.06E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 2/10/1992 1.94E-16 S.OOE-12 1.25E-12 4.28E-17 8.00E-14 2.00E-14 4.08E-17 ,2.00E-12 5.00E-13 3.51E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 5/11/1992 2.54E-16 S.OOE-12 1.25E-12 6.49E-16 8.00E-14 2.00E·14 6.86E-17 2.00E-12 5.00E-13 1.38E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/10/1992 1.73E-16 S.OOE-12 1.25E-12 1.55E-16 8.00E-14 2.00E-14 1.20E-16 2.00E-12 5.00E-13 1.53E-14 4.00E-12 l.OOE-12 Not Analyzed Not AJ1plicable Not Applicable 11/9/1992 1.56E-16 S.OOE-11 1.25E-12 3.19E-17 S.OOE-14 2.00E-14 4.90E-18 l.OOE-12 S.OOE-13 1.86E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/9/1993 2.10E-16 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 3.89E-17 Z.OOE-12 5.00E-13 2.52E-14 4.00E·12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/10/1993 1.00E-16 S.OOE-12 1.25E-12 4.11E-17 8.00E-14 2.00E-14 6.43E-17 2.00E-12 5.00E-13 1.26E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/10/1993 2.30E-16 ~.OOE-12 1.25E-12 6.00E-17 8.00E-14 2.00E-14 6.43E-17 2.00E·12 5.00E-13 1.60E-14 4.00E·12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/8/1993 S.OOE-12 . 1.25E-12 8.00E-14 2.00E-14 O.OOE+OO _ 2.()0E-12 5.00E-13 1.57E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable Date Effluent 9E-14 uCi/ml BHV-1U I Effluent 2E-14 uCi/ml BHV-1T230 Effluent j~E-13 uCi/ml -BHV-1R Effluent 6E-13 uCi/ml BHV-1PB Effluent 4e-15 uCi/ml BHV-1T232 Concentration Concentration C!oncentration Concentration Concentration Limit= Limit= Limit= Limit= Limit= - AlARAGoal= 2.25E-14 uCi/ml ALARA Goal= SE-15 uCi/ml AlARAGoal= Z.25E-13 uCi/ml ALARAGoal = l.SE-13 uCi/ml AlARAGoal= 1E-15 uCi/ml Pre 1994MPC SE-12 uCi/inl Pre 1994 MPC SE-14 uCi/ml Pre 1994 MPC ZE-12 uCi/ml Pre 1994 MPC 4E-1Z uCi/ml Pre 1994 MPC Not Applicable Limit= Limit= limit= Limit= Limit= I .. Pre 1994 1.25E-12 uCi/ml I Pre 1994 SE-13 uCi/ml Pre 1994 1E-1Z uCi/ml Pre 1994 Not Applicable I AlARAGOAL= ALARAGOAL= ALARAGOAL= ALARAGOAL=i Cone -EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone I'FC EFCA 2/7/1994 1.82E-16 S.OOE-12 1.25E-12 S.OOE-18 8.00E-14 2.00E-14 <1.30E-17 2.00E-12 S.OOE-13 2.59E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/9/1994 3.60E-16 S.OOE-12 1.25E-12 2.70E-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 S.OOE-13 1.60E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/9/1994 4.04E·16 5.00E-12 '1.25E-12 2.70E-16 8.00E-14 2.00E-14 .2.94E-16 2.00E·12 5.00E-13 2.00E-15 4.00E-12 l.OOE-12 Not Anallf!'ed Not Applicable • Not Applicable 11/7/1994 9.18E-17 S.OOE-12 l.25E·12 o.60E-16 8.00E-14 2.00E-14 2.91E-16 2.00E·12 S.OOE-13 2.00E-15 4.00E-12 l.OOE-12 t-~ot Analyzed Not Applicable Not Applicable 2/7/1995 .1.77E-16 9.00E-14 2.25E-14. 9.70E-17 2.00E-14 5.00E-15 9.70E-17 9.00E-13 "2.25E-13 8.60E-15 6.00E-13 1.50E-13 Not Analyzed · Not Applicable Not Applicable 5/9/1995 9.40E·17 9.00E-14 2.25E-14 5.36E-16 2.00E-14 S.OOE-15 1.60E-15 9.00E-13 2.25E-13 3.84E-15 6.00E-13 l.SOE-13 'Not Analyzed Not Applicable Not Applicable 8/9/1995 2.70E-16 9.00E-14 2.25E-14' 1.60E-16 2.00E-14 5.00E-15 2.76E-16 9.00E-13 2.25E-13 3.76E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 11/11/1995 4.80E-15 9.00E·14 2.25E-14 6.41E·16 2.00E-14 5.00E-15 8.93E-16 9.00E-13 2.25E·13 5.20E-15 6.00E·13 1.50E-13 Not Analyzed Not Applicable Not Applicable 2/5/1996 5.34E·15 9.00E-14 g,z5E-14 2.30E-15 2.00E-14 S.OOE-15 1.30E·15 9.00E-13 2.25E-13 4.20E-15 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 5/6/1996 S.llE-16 9.00E-14 2.25E-14 3.06E-16 2.00E-14 S.OOE-15 1.40E-16 .9.00E-13 2.25E-13 7.03E-15 6 .. 00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 8/5/1996 5.99E-16 9.00E-14 2.25E·14 1.55E-15 2.00E-14 5.00E-15 2.03E-16 9.00E-13 :Z.25E·13 5.94E-15 6.00E·13 1.50E-13 Nat Analyzed Not Applicable _Not AQplicable 11/6/1996 3.38E·16 9.00E-1_4 2.25E-14 5.45E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.22E-14 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 2/6/1997 l.OOE-16 9.00E-14 2.25E-14 1.25E-16 2.00E-14 5.00E-15 1.28E-16 ~.OOE-13 2.25E-13 5.68E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 5/5/1997 1.09E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 4.39E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 8/11/1997 2.88E-16 9.00E-14 2.25E-14 3.83E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E·13 5.29E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 1/5/1998 3.24E·16 9.00E-14 , 2.25E-14 3.47E-16 2.00E-14 5.00E-15 1.19E-16 . 9.00E-13 2.25E-13 4.73E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable-Not Applicable 4/28/1998 4.75E·16 9.00E-14 2.25E-14 6.73E-16 2.00E-14 5,00E-15 5.69E-16 9.00E-13 2.25E-13 5.94E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/31/1998 8.84E-16 9.00E-14 ·· 2.25E-14 1.93E-15 2.00E-14 5.00E-15 1.43E-15 9.00E·13 2.25E-13 5.22E·15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/28/1998 2.81E-16 9.00E-14 2.25E-14 2.89E-16 2.00E-14 5.00E-15 1.80E-16 9.00E-13 2.25E-13 4.64E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/28/1998 g.08E-16 9.00E-14 2.25E-14 4.93E-16 2.00E-14 5.00E-15 5.01E·16 9.00E-13 2.25E-13 1.06E-14 6.00E-13 1.50E-13 Not Analyzed Not Ap_plicable Not ApQiicable _j 3/29/1999 2.06E-16 9.00E-14 2.25E-14 2.06E-16 2.00E-14 5.00E-15 1.42E-16 9.00E-13 2.25E-13 6.69E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/3/1999 5.31E-16 9.00E·14 2.25E-14 2.47E-16 2.00E-14 5.00E-15 2.23E-16 9.00E-13 2.25E·13 6.44E-15 6.00E·13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/27/1999 8.98E-16 9.00E-14 2.25E-14 3.90E-16 2.00E-14 5.00E-15 2.96E-16 9.00E-13 2.25E-13 7.29E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/28/1999 1.48E-15 s.OOE-14 ,2.25E-14 6.00E-16 2.00E-14 5.00E-15 5.57E·16 9.00E·13 2.25E-13 6.19E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/27/2000 1.00E-16 s,ooE-14 2.25E-14 1.06E-16 2.00E·14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.23E-15 6.00E-13 1.50E-13 Not AnaJyzed Not Applicable ·· Not Applicable 6/26/2000 3.47E-16 9.00E-14 2.25E-14 3.46E-16 2.00E-14 5.00E-15 3.62E-16 9.00E-13 2.25E-13 4.50E-15 6.00E-13 1.50E-13 Not AnaJyzed Not Applicable Not Applicable 9/26/2000 2.51E-16 .9.00E-14 • 2.25E-14 1.78E-16 2.00E-14 5.00E-15 3.25E-16 9.00E-13 2.25E-13 8.55E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Apl2!lcable 12/26/2000 1.00E-16 9.00E-14 I 2.25E-14 1.42E-16 2.00E-14 5.00E-15 1.31E·16 9.00E-13 2.25E-13 7.77E-15 6.00E·13 1.50E·13 Not Analyzed Not Applicable Not Applicable 3/26/2001 ~.10E-16 9.00E-14 2.25E-14 l.OOE-15 2.00E-14 5.00E-15 .l.OOE-15 9.00E-13 2.25E-13 7.19E-15 6.00E-13 1.50E-13 Not Analyzed , Not Applicable Not Applicable 7/29/2001 1.52E-16 9.00E-14 . 2.25E-14 1.44E-16 2.00E-14 5.00E-15 1.77E-16 9.00E-13 ·2.25E-13 7.21E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable ])lot Applicable 9/24/2001 1.03E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.09E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable jllot Applicable 12/31/2001 l.OOE-16 . 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.39E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable . Not Applicable 4/1/2002 2.05E-16 9.00E-14 2.25E-14 2.44E-16 2.00E-14 5.00E-15 :Z.29E-16 9.00E-13 2.25E-13 8.15E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not A{lll.licable -7/1/2002 3.55E-16 S.OOE-14 2.25E-14 4.85E-16 2.00E-14 5.00E-15 1.06E-16 9.00E-13 2.25E-13 7.65E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not ApJJiicable 9/30/2002 1.17E-16 ~.OOE-14 2.25E·14 1.61E-16 LOOE-14 5.00E-15 .l.OOE-16 9.00E-13 2.25E-13 3.68E-15 6.00E·13 1.SOE·13 Not Analyzed Not Applicable Not Applicable 12/30/2002 1.00E·16 9.00E-14 2.25E·14 1.03E-16 '2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 9.46E-15 6.00E-13 L50E-13 Not Analyzed • Not Applicable ' Not Applicable 3/31/2003 l..20E·16 9.00E-14 2.25E-14 1.12E-16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 4.68E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2003 2.18E-16 9.00E-14 2.25E-14 3.40E-16 2.00E-14 5,00E-15 1.67E·16 9.00E·13 2.25E·13 5.96E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable : Not Applicable 9/29/2003 l.OOE-16 9.00E-14 ·2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.28E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable jllot Applicable 12/29/2003 1.00E-16 g.OOE-14 2.25E·14 2.54E-16 2.00E-14 5,00E-15 ;3.35E-16 9.00E-13 2.25E-13 6,25E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable l\lot Applicable 3/29/2004 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 .l.OOE-16 9.00E-13 2.25E-13 1.54E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/27/2004 l.OOE-16 g.OOE-14 2.25E-14 l.OOE-16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 3,04E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not App_licable 9/27/2004 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5,00E-15 1.00E-16 9.00E-13 2.25E-13 1.05E-14 6.00E-13 l.SOE-13 Not Analyzed ' Not Applicable Not Applicable 12/27/2004 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.59E-14 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 3/28/2005 1.00E-16 g.OOE-14 _2.25E-14 l.OOE-16 LOOE-14 5,00E-15 .l.OOE-16 . 9.00E-13 2.25E·13 7.42E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable • Not Applicable 6/29/2005 1.00E-16 9.00E-14 2.25E-14 1.30E-16 2.00E-14 5.00E-15 1.20E-16 9.00E-13 2.25E·13 7.94E-15 6.00E-13 1.50E-13 Not Analyzed , Not Applicable jllot Applicable 9/26/2005 1.00E-16 9.00E-14 2.25E-14 2.56E-16 2.00E-14 5,00E-15 2.42E-16 9.00E-13 2.25E-13 1.22E·14 6.00E-13 1.SOE-13 Not Analyzed jllot Applicable Not Applicable 1/3/2006 2.13E-16 9.00E-14 2.25E-14 1.04E·16 2.00E-14 5.00E-15 l.OOE-16 9.00E·13 2.25E-13 3.73E-14 6.00E-13 1.50E·13 Not Analyzed Not Applicable Not Applicable 4/3/2006 1.62E-16 9.00E-14 2.25E-14 1.86E-16 2.00E-14 5.00E·15 l.OOE-16 9.00E-13 2.25E·l3 8.36E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/3/2006 1.86E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 j 9.00E-13 2.25E-13 9.77E-15 6.00E-13 1.50E·13 Not Analyzed ~t Applicable Not Applicable Date Effluent 9E-14 uCi/ml BHV-1U Effluent ZE-14 uCi/ml BHV-1T230 Effluent 9E-13 uCi/ml BHV-1R Effluent 6E-13 uCi/ml BHV-1PB Effluent 4e-15 uCi/ml BHV-1T232 Concentration Concentration Concentration Concentration Concentration Limit= Limit= limit= Limit= limit= ALARA Goal -1 2.25E-14 uCi/ml ALARA Goal= SE-15 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARA Goal-1.SE-13 uCi/ml ALARAGoal = 1E-15 uCi/ml Pre 1994 MPC SE-12 uCi/ml Pre 1994 MPC SE-14 uCi/ml Pre 1994 MPC 2E-12 uCi/ml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable Limit= limit= Limit= Limit= limit= - pre1994 1.2SE-12 uCi/inl Pre 1994 SE-13 uCi/ml Pre 1994 1E-12 uCi/ml Pre 1994 Not Applicable ALARAGOAL= ALARAGOAL= ALARAGOAL= ALARAGOAL= Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 10/2/2006 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 1.30E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 1/1/2007 l.OOE-16 9.00E-14 2.25E·14 1.47E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.17E-14 6.00E-13 1.50E·13 Not Analyzed Not Applicable Not Applicable 4/2/2007 2.23E-16 ~.OOE-14 2.25E-14 1.63E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.65E-14 6.00E-13 1.50E-13 Not Analyzed Not ~plicable Not Applicable 7/2/2007 3.35E-16 S.OOE-14 2.25E·14 1.34E-16 2.00E-14 5.00E-15 1.36E-16 9.00E-13 2.25E-13 1.78E-14 6.00E-13 1.50E-13 Not Ana!Yzed Not Applicable Not Applicable 9/30/2007 1.15E-16 S.OOE-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 ,l.OOE-16 9.00E-13 2.25E-13 7.68E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/31/2007 l.OOE-16 l B.OOE-14 2.25E-14 1.93E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 l.SOE-13 Not Analyzed !'Jot Applicable Not Applicable 3/31/2008 1.14E-16 S.OOE-14 2.25E-14 1.13E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E·13 6.44E-15 6.00E-13 1.50E-13 Not Analyzed !'Jot Applicable Not Applicable 6/30/2008 7.09E-16 9.0QE-14 2.25E-14 3,83E-16 2.00E-14 5.00E-15 ~.27E-16 9.00E-13 2.25E-13 6.52E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable . Not Applicable 9/30/2008 7.69E-16 9.00E-14 2.25E-14 2.94E-16 2.00E-14 S.OOE-15 1.90E-16 9.00E-13 2.25E-13 7.64E-15 6,00E-13 1.50E-13 Not Analyzed !'Jot Applicable Not Applicable 12/31/2008 1.21E-15 9.00E-14 2.25E-14 4.76E-16 2.00E-14 5.00E-15 3.34E-16 9.00E-13 2.25E-13 1.16E-14 6,00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/15/2009 2.14E-15 9.00E-14 2.25E-14 1.02E-15 2.00E-14 5.00E-15 l.OOE-15 9.00E-13 2.25E-13 4.44E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/15/2009 5.97E-17 9.00E-14 2.25E-14 2.35E-16 2.00E-14 5.00E-15 2.18E-16 9.00E-13 2.25E·13 5.13E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/15/2009 9.55E-16 9.00E-14 2.25E-14 1.71E-16 2.00E-14 5.00E-15 9.87E-17 9.00E-13 2.25E-13 9.47E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/15/2009 1.24E-15 9.00E-14 2.25E-14 9.25E-17 2.00E-14 5.00E-15 5.60E-17 9.00E-13 2.25E-13 5.95E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/31/2010 1.97E-15 9.00E-14 . 2.25E-14 2.15E-16 2.00E-14 5.00E-15 3.27E-16 9.00E-13 2.25E-13 l.OOE-14 6,00E-13 l.SOE-13 Not Analyzed Not AI!Piicable Not Applicable -6/30/2010 1.58E-15 9.00E-14 2.25E·14 4.71E-16 2.00E-14 5.00E-15 7.70E-16 9.00E-13 2.25E-13 4.07E-15 6.00E-13 l.SOE-13 Not AnaJyzed Not Applicable Not Applicable 9/30/2010 8.42E-16 9.00E-14 2.25E-14 2.80E-16 2.00E-14 S.OOE-15 1.31E-16 9.00E-13 2.25E·13 6.80E-15 6.00E-13 1,50E-13 Not Analyzed Not Applicable Not Applicable 12/31/2010 1.27E-15 9.00E-14 2.25E-14 2.32E-16 Z.OOE-14 S.OOE-15 2.30E-16 9.00E-13 2.25E-13 1.27E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/4/2011 9.01E-16 9.00E-14 2.25E-14 1.90E-16 2.00E-14 5,00E-15 3.64E-16 9.00E-13 2.25E-13 1.09E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/4/2011 1.59E-15 9.00E-14 2.25E-14 5.31E-16 2.00E-14 5.00E-15 4.99E-16 9.00E-13 2.25E-13 8.38E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 10/3/2011 2.92E-16 9.00E-14 2.25E-14 1.17E-16 2.00E-14 5.00E-15 6.76E-17 9.00E-13 2.25E-13 1.14E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 1/3/2012 6.73E-16 9.00E-14 2.25E·14 1.19E-16 2.00E-14 5.00E-15 8.58E-17 9.00E-13 2.25E-13 1.73E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/3/2012 7.87E-16 9.00E-14 2.25E-14 2.64E-16 2.00E-14 S,OOE-15 3.95E-16 9.00E-13 2.25E-13 1.25E-14 6.00E-13 1.SOE-13 Not Analyzed Not Applicable Not ApJ>Iicable 7/2/2012 1.86E-15 9.00E-14 2.25E-14 8.33E-16 2.00E-14 5,00E-15 9.85E-16 9.00E-13 2.25E-13 9.55E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 10/1/2012 1.06E-15 9.00E-14 2.25E-14 2.11E-16 2 OOE-14 5.00E-15 2.34E-16 9.00E-13 2.25E-13 l.BE-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12}31/2012 6.86E-16 9.00E-14 2.25E-14 1.27E-16 2.00E-14 5.00E-15 1.38E-16 9.00E-13 2.25E-13 1.54E-14 G.OOE-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/25/2013 9.91E-16 9.00E-14 2.25E·14 1.86E-16 2.00E-14 5.00E-15 l.04E-16 9.00E-13 2.25E-13 1.82E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/2/2013 1.46E-16 9.00E-14 2.25E-14 3.34E-16 2.00E-14 5.00E-15 3.91E-16 9.00E-13 2.25E-13 5.78E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/30/2013 ~.89E-16 9.00E-14 2.25E-14 9.13E-17 2.00E-14 5.00E-15 1.05E-16 9.00E-13 2.25E-13 8.00E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/30/2013 5.21E-16 9.00E-14 2.25E-14 4.34E-17 2.00E-14 S.OOE-15 3.70E-17 9.00E-13 2.25E-13 2.59E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/31/2014 1.07E-15 9.00E-14 2.25E·14 2.07E-16 2.00E-14 S.OOE-15 3.69E-16 9.00E-13 2.25E-13 1.24E-14 G.OOE-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2014 2.24E-15 9.00E-14 2.25E-14 5.14E-16 2.00E-14 S.OOE-15 1.09E-15 9.00E-13 2.25E-13 1.23E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/30/2014 1.59E-15 9.00E-14 2.25E-14 2.00E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.39E-14 6.00E-13 1.50E-13 :l.OOE-16 1 4.00E-15 1.00E-15 12/29/2014 2.00E-16 9.00E-14 2.25E-14 S.OOE-17 2.00E-14 S.OOE-15 7.00E-17 9.00E-13 2.25E-13 2.00E-14 6.00E-13 1.50E-13 7.00E-18 4.00E-15 l.OOE-15 3/30/2015 1.90E-15 9.00E-14 2.25E-14 3.00E-17 2.00E-14 5.00E-15 6.00E-17 9.00E-13 2.25E-13 2.80E-14 6.00E-13 1,50E-13 4.00E-18 4.00E-15 1.00E-15 6/29/2015 6.00E-16 9.00E-14 2.25E-14 2.00E-16 2.00E-14 5.00E·15 7.00E-16 9.00E-13 2.25E-13 9.00E-15 6.00E-13 1.50E-13 l.OOE-17 4.00E-15 l.OOE-15 9/28/2015 '1.60E-15 9.00E-14 I 2.25E-14 8.00E-17 2.00E-14 S.OOE-15 6.00E-16 9.00E-13 2.25E-13 1.00E-14 6.00E-13 l.SOE-13 7.00E-18 4.00E-15 l.OOE-15 12/28/2015 2.20E-16 9.00E-14 2.25E-14 5.00E-17 2.00E-14 5.00E-15 2.00E-16 9.00E-13 2.25E-13 1.20E-14 6.00E-13 1.50E-13 l.OOE-18 4.00E-15 l.OOE·15 3/28/2016 2.00E-16 9.00E-14 2.25E-14 3.00E-17 2.00E-14 5.00E-15 3.00E-16 9.00E-13 ~.25E-13 1.40E-14 6.00E-13 1.50E-13 2.00E-18 4.00E-15 l.OOE-15 6/27/2016 1.10E-15 9.00E-14 2.25E-14 7.00E-17 2.00E-14 5.00E·15 9.00E-16 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C! ..-.- - 1/) c 0 ~ -c (I) u c 0 0 N M N I E :::J "i: 0 .c 1-,.... ::> J: m 'E -C3 :I It) .... I w '<t 11 - :<:::: E .§~ ...J :I C it) 0 ..- ·-I ~~ ..... r::..-B II :S iii u <3 "E < Gl a: 2 < -...J iii < I I "'<t 0 I UJ 0 C! ...- I I I I LO (!) t--a:> O'l 0 0 0 0 0 I I I I I UJ UJ UJ UJ UJ 0 0 0 0 0 C! C! C! C! C! ...-,.... I 0 C\1 M "'<t LO ..... ...-...-...-...-...- I I w I I I UJ UJ UJ UJ UJ 0 0 0 0 0 0 C! 0 C! 0 C! C! 1are~§ Bo1f '/ ~~~ I (!) t--a:> ..... .... I w I UJ UJ 0 0 0 C! C! C! ...- 9~-~aa 9 ~-liON 9~-PO 9~-das 9 ~ -Bny 9~-unr 9 ~ -keV'J 9 ~ -Jd'v' 9 ~ -JBV'J 9 ~-qa::J 9 ~-uer g~-~aa g~-IION 9~-PO g ~-des g ~ -Bny g~-1nr g ~-unr g ~ -ABV'J g ~ -Jd'v' g ~-uer v ~-oaa v ~-liON v~-PO v~-das TAB2 BHV -2 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent 9E-14 uCi/ml BHV-2U Effluent 2E-14 uCi/ml BHV-2T230 Effluent 9E-15 uCi/ml BHV-2R Effluent 6E-13 uCi/ml BHV-2PB Effluent 4e-15 uCi/ml BHV-2T232 Concentration Concentration Concentration Concentration Concentration Limit= Limit= Limit= Limit= Limit= - ALARAGoal-2.25E-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARA Goal-l.SE-13 uCi/ml ALARA Goal -, 1E-15 uCi/ml Pre 1994 MPC SE-12 uCi/ml Pre 1994 MPC BE-14 uCi/ml Pre 1994 MPC 2E-12 uCi/ml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable I Limit= limit= Limit= Limit= limit== Pre 1994 ALARA 1.2SE-12 uCi/ml Pre 1994 SE-13 uCi/ml Pre 1994 1E-12 uCi/ml Pre 1994 Not Applicable GOAL= ALARAGOAL= ALARAGOAL= /ILARAGOAL= Cone EFC ~FCA Cone EFC EFCA Cone 'EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 1.39E-15 S.OOE-12 1.25E-12 3.69E-16 8.00E-14 2.00E-14 5.92E-16 2.00E-12 5.00E-13 1.67E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 12/14/1981 4.62E-16 S.OOE-12 '1.25E-12 8.03E-16 8.00E-14 2.00E-14 3.62E-16 2.00E-12 S.OOE-13 1.33E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 3/29/1982 7.07E-16 S.OOE-12 1.25E-12 1.10E-15 8.00E-14 2.00E-14 7.27E-16 2.00E-12 5.00E-13 1.52E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 6/30/1982 8.84E-16 -S.OOE-12 1.25E-12 7.73E-16 8.00E-14 2.00E-14 4.78E-16 2.00E-12 S.OOE-13 1.98E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 9/27/1982 1.23E-15 5.00E-12 1.25E-12 3.60E-16 8.00E-14 2.00E-14 8.73E-16 2.00E-12 S.OOE-13 2.35E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Npt Applicable 1/3/1983 2.64E-15 5.00E-12 1.25E-12 2.55E-16 8.00E-14 2.00E-14 1.98E-16 2.00E-12 5.00E-13 2.85E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 4/4/1983 2.14E-16 5.00E-12 1.25E-12' l.OlE-16 8.00E-14 2.00E-14 1.57E-16 ~.OOE-12 S.OOE-13 2.48E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 6/30/1983 ~.85E-16 5.00E-12 1.25E-12 2.06E-16 8.00E-14 2.00E-14 2.24E-16 2.00E-12 5.00E-13 1.79E-14 4.00E-12 l.OOE-12 ,Not Analyzed Not Applicable Not Applicable 10/3/1983 2.70E-16 5.00E-12 ,1.25E-12 3.36E-16 8.00E-14 2.00E-14 4.37E-16 2.00E-12 5.00E-13 1.78E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not A.QQiicable 1/3/1984 2.78E-15 5.00E-12 1.25E-12 1.20E-16 8.00E-14 2.00E-14 6.64E-17 2.00E-12 5.00E-13 9,14E-15 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable -4/2/1984 4.28E-16 5.00E-12 1.25E-12 1.75E-16 B.OOE-14 2.00E-14 4.57E-17 2.00E-12 5.00E-13 3.55E-14 4.00E-12 l.OOE-12 Not AnaiY):ed Not Applicable Not Applicable 7/2/1984 2.78E-15 S.OOE-12 1.25E-12 8.12E-16 8.00E-14 2.00E-14 1.98E-16 2.00E-12 5.00E-13 1.68E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 10/1/1984 2.69E-16 S.OOE-12 1.25E-12 2.66E-17 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 5.00E-13 1.77E-14 4.00E-12 l.OOE-12 Not Allaiyzed Not Applicable Not A.Qplicable 1/2/1985 2.15E-16 S.OOE-12 1.25E-12 7.55E-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 S.OOE-13 3.19E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 4/1/1985 1.00E-16 5.00E-12 1.25E-12 1.67E-16 8.00E-14 2,00E-14 6.75E-17 2.00E-12 5.00E-13 7.56E-15 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 7/1/1985 3.70E-17 5.00E-12 1.25E-12 9.00E-16 8.00E-14 2.00E-14 4.90E-17 2.00E-12 5.00E-13 1.31E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable _Not Applicable 9/30/1985 9.32E-17 S.OOE-12 1.25E-12 2.18E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 5.00E-13 3.64E-15 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 1/2/1986 l.OOE-16 5.00E-12 -l.25E-12 2.16E-16 8.00E-14 2.00E-14 2.15E-17 2.00E-12 S.OOE-13 3.04E-16 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 4/1/1986 1.31E-15 5.00E-12 1.25E-12 l.SOE-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 5.00E-13 2.90E-15 4.00E-12 l.OOE-12 Not Analyzed Not ARPiicable Not Applicable 6/30/1986 2.23E-16 S.OOE-12 ' 1.25E-12 1.32E-16 8.00E-14 2.00E-14 7.09E-17 2.00E-12 5.00E-13 2.53E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 10/27/1986 6.41E-16 S.OOE-12 1.25E-12 1.74E-16 8.00E-14 2.00E-14 3.67E-16 2.00E-12 5.00E-13 1.04E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable !'4ot Applicable 12/15/1986 3.56E-16 S.OOE-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 1.05E-16 2.00E-12 5.00E-13 7.81E-15 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 3/16/1987 5.31E-16 S.OOE-12 1.25E-12 1.30E-16 8.00E-14 2.00E-14 7.74E-17 2.00E-12 5.00E-13 J .80E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/11/1987 4.06E-16 S.OOE-12 1.25E-12 6.63E-17 8.00E-14 2.00E-14 1.34E-16 2.00E-12 5.00E-13 l.lOE-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 9/9/1987 2.74E-16 S.OOE-12 1.25E-12 2.38E-16 8.00E-14 2.00E-14 '1.38E-16 2.00E-12 S.OOE-13 1.04E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 11/2/1987 3.73E-16 5.00E-12 1.25E-12 3.11E-16 8.00E-14 2.00E-14 ,1.83E-16 2.00E-12 fi.OOE-13 1.17E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not ~plicable 2/16/1988 2.78E-15 S.OOE-12 1.25E-12 2.31E-17 8.00E-14 2.00E-14 1.20E-16 2.00E-12 5.00E-13 3.55E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 5/18/1988 4.63E-16 S.OOE-12 1.25E-12 1.49E-16 8.00E-14 2.00E-14 UOE-16 2.00E-12 S.OOE-13 1.18E-14 4.00E-12 1.00E-12 ,Not Analyzed Not Applicable Not Applicable 8/15/1988 8.06E-16 S.OOE-12 1.25E-12 8.69E-16 8,00E-14 2.00E-14 1.80E-16 2.00E-12 5.00E-13 1.42E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/14/1988 4.34E-16 5.00E-12 1.25E-12 6.76E-16 8.00E-14 2.00E-14 1.57E-16 2.00E-12 5.00E-13 2.25E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/13/1989 5.80E-16 5.00E-12 1.25E-12 2.85E-16 8.00E-14 2.00E-14 1.55E-16 2.00E-12 5.00E-13 2.80E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/15/1989 5.06E-16 5.00E-12 1.25E-12 2.28E-16 8.00E-14 2.00E-14 1.63E-16 2.00E-12 5.00E-13 6.05E-15 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/14/1989 4.71E-16 S.OOE-12 1.25E-12 9.60E-16 8,00E-14 2.00E-14 L26E-15 2.00E-12 5.00E-13 6.65E-15 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/13/1989 1.14E-15 5.00E-12 1.25E-12 4.08E-16 8.00E-14 2.00E-14 4,18E-16 2.00E-12 5.00E-13 1.59E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/12/1990 1.09E-15 5.00E-12 1.25E-12 3.25E-16 8.00E-14 2.00E-14 3.74E-16 2.00E-12 5.00E-13 1.98E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/14/1990 9.32E-16 ·s.OOE-12 ~.25E-12 5.27E-16 8.00E-14 2.00E-14 3.97E-16 2.00E-12 ·s.OOE-13 1.69E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/13/1990 1.66E-16 S.OOE-12 1.25E-12 5.49E-16 8.00E-14 2.00E-14 4.75E-17 2.00E-12 S.OOE-13 1.27E-15 4.00E-12 l.OOE-12 !'4ot AnaLyzed Not Applicable Not Applicable 11/12/1990 6.05E-16 S.OOE-12 1.25E-12 2.64E-16 8.00E-14 2.00E-14 1.93E-16 2.00E-12 S.OOE-13 2.25E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/11/1991 8.72E-17 5.00E-12 1,.25E-12 7.00E-18 S.OOE-14 2.00E-14 3.33E-17 2.00E-12 S.OOE-13 3.49E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/13/1991 1.16E-16 5.00E-12 1.25E-12 3.86E-16 8.00E-14 2.00E-14 2.80E-16 2.00E-12 5.00E-13 1.50E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/12/1991 9.02E-17 5.00E-12 1.25E-12 8.82E-17 8.00E-14 2.00E-14 7.65E-17 2.00E-12 5.00E-13 1.58E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/11/1991 4.81E-17 5.00E-12 1.25E-12 3.82E-17 8.00E-14 2.00E-14 2.54E-17 2.00E-12 5.00E-13 1.45E-14 4.00E-12 l.OOE-12 Not Analyzed Not Ap[>licable Not Applicable 2/10/1992 1.54E-16 S.OOE-12 '1.25E-12 6.82E-17 B.OOE-14 2.00E-14 1.40E-17 2.00E-12 5.00E-13 3.41E-14 4.00E-12 l.OOE-12 Not Analyzed ·Not Applicable Not Applicable S/11/1992 2.38E-16 5.00E-12 1.25E-12 7.63E-17 8.00E-14 2.00E-14 3.07E-17 2.00E-12 5.00E-13 1.27E-14 4.00E-12 l.OOE-12 Not Analyzed Not ApJlllcible Not Applicable 8/10/1992 1.01E-16 S.OOE-12 1.25E-12 7.07E-17 8.00E-14 2.00E-14 2.80E-17 2.00E-12 5.00E-13 1.41E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/9/1992 5.20E-17 S.OOE-12 1.25E-12 3.65E-17 8.00E-14 2.00E-14 1.78E-17 2.00E-12 5.00E-13 1.71E-14 4.00E-12 l.OOE-12 Not Analyzed (llot Applicable !'4ot Applicable 2/9/1993 2 39E-16 S.OOE-12 1.25E-12 2.97E-17 8.00E-14 2.00E-14 6.31E-17 2.00E-12 S.OOE-13 3.41E-14 4.00E-12 l.OOE-12 Not Analyzed j\lot Applicable Not Applicable 5/10/1993 1.00E-16 S.OOE-12 1.25E-12 7.11E-17 8.00E-14 2.00E-14 3.19E-17 2.00E-12 5.00E-13 1.34E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/10/1993 1.90E-16 5.00E-12 1.25E-12 l.OOE·16 8.00E-14 2,00E-14 l.OOE-16 2.00E-12 S.OOE-13 1.80E-14 4.00E-12 1.00E-12 !'lot Analyzed Not Applicable Not Applicable -- Date Effluent 9E-14 uCi]ml BHV-2U ' Effluent ZE-14 uCi/ml BHV-2T230 'Effluent 9E-15 uCi/ml BHV-2R Effluent 6E-13 uCi/ml BHV-2PB Effluent 4e-15 uCi/ml BHV-2T232 Concentration Concentration Concentration Concentration Concentration Limit= Limit= Limit= Limit= Limit= AlARAGoal = 2.25E-14 uCi/ml ALARAGoal = SE-13 uCi/ml AlARAGoal = 2.25E-13 uCi/ml ALARA Goal= l.SE-13 uCi/ml AlARAGoal = 1E-15 uCijml I Pre 1994MPC SE-12 uCi/ml Pre 1994 MPC BE-14 uCi/ml Pre 1994 I\IIPC 2E-12 uCi/ml Pre 1994 MPC .4E-12 uCi/ml Pre 1994 MPC Not Applicable I Limit= Limit= Limit= Limit= Limit= - I Pre 1994 ALARA 1.25E-12 uCi/ml Pre 1994 SE-13 uCi/ml Pre 1994 lE-12 uCi/ml Pre 1994 Not Applicable GOAL= ALARAGOAL= ALARAGOAL= ALARAGOAL= I Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 11/8/1993 l.OOE-16 S.OOE-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-13 1.49E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/7/1994 2.23E-16 5.00E-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 1.84E-16 2.00E-12 5.00E-13 2.19E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not ARplicable 5/9/1994 2.16E-16 5.00E-12 1.25E-12 7.20E-17 8.00E-14 2.00E-14 9.89E-17 2.00E-12 5.00E-13 1.37E-14 4.00E-12 l.OOE-12 Not Analyzed Not ApQ_Iicable Not A(lQiicable 8/9/1994 iJ.29E-17 5.00E-12 i.25E-12 2.96E-16 8.00E-14 2.00E-14 3.04E-16 2.00E-12 5.00E-13 l.OOE-16 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/7/1994 9.21E-17 5.00E-12 1.25E-12 2.35E-16 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 5.00E-13 l.OOE-16 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/7/1995 1.18E-16 9.00E-14 2.25E-14 9.70E-17 2.00E-14 5.00E-15 9.70E-17 9.00E-13 2.25E-13 7.42E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable " 5/9/1995 9.40E-17 9.00E-14 2.25E-14 1.20E-16 2.00E-14 5.00E-15 3.50E-16 9.00E-13 2.25E-13 3.90E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 8/9/1995 8.90E-17 9.00E-14 2.25E-14 9.67E-17 2.00E-14 5.00E-15 1.35E-16 9.00E-13 2.25E-13 2.38E-16 6.00E-13 1.50E-13 Not Anajyzed Not Applicable Not Applicable 11/11/1995 2.83E-15 9.00E-14 2.25E-14 4.09E-16 2.00E-14 5.00E-15 5.23E-16 9.00E-13 2.25E-13 6.77E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable !)Jot Applicable - 2/5/1996 1.75E-15 !l.OOE-14 2.25E-14 8.66E-16 2.00E-14 5,00E-15 4.86E-16 9.00E-13 2.25E-13 3,50E-15 6,00E-13 1,50E-13 IIJot Analyzed i)lot Applicable ' Not Applicable 5/6/1996 1.40E-16 . 9.00E-14 2.25E-14 1.15E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.85E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 8/5/1996 1.43E-16 9.00E-14 ,2.25E-14 2,78E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 5.83E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable f\!ot Applicable 11/6/1996 1.45E-16 : 9.00E-14 2.25E-14 1.57E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.19E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 2/6/1997 1.00E-16 ll-OOE-14 2.25E-14 1,00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 5.84E-16 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 5/5/1997 l.OOE-16 . 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 3.89E-15 6.00E-13 1.50E-13 Not Analyzed • Not Applicable : Not Applicable 8/11/1997 l.OOE:16 9.00E-14 2.25E-14 1.09E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 5.69E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 1/5/1998 f.55E-16 '9.00E-14 ~.25E-14 1,07E-16 2.00E-14 5.00E-15 5.00E-17 9.00E-13 2.25E-13 5.11E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/28/1998 1.20E-16 9.00E-14 2.25E-14 1.71E-16 l.OOE-14 5.00E-15 1.28E-16 9.00E-13 :?.25E-13 6.40E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable I Not Applicable 7/31/1998 1.47E-16 : 9.00E-14 .2.25E-14 4.24E-16 Z.OOE-14 5.00E-15 3.39E-16 9.00E-13 2.25E-13 4.80E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable !)Jot Applicable 9/28/1998 1.00E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 4.26E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/28/1998 2.54E-16 fl.OOE-14 2.25E-14 2.15E-16 2.00E-14 5.00E-15 1.38E-16 9.00E-13 2.25E-13 6.88E-15 6.00E-13 1,50E-13 Not Analyzed Not Applicable NOt Applicable 3/29/1999 1.07E-16 '9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.61E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/3/1999 2.46E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 :LOOE-16 9.00E-13 2.25E-13 6.95E-15 6.00E-13 1.50E-13 Not Analyzed NOt A(lplicable Not AQ_plicable 9/27/1999 2.81E-16 9.00E-14 2.25E-14-1.41E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.35E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable ~ Not Applicable 12/28/1999 5.20E-16 .9.00E-14 2.25E-14 2.60E-16 2.00E-14 5.00E-15 2.01E-16 9.00E-13 2.25E-13 7.00E-15 6.00E-13 1,50E-13 Not Analyzed Not Applicable Not Applicable 3/27/2000 1.00E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 :LOOE-16 9.00E-13 2.25E-13 7.12E-15 6.00E-13 1.50E-13 Not Analyzed Not AP.plicable Not Applicable 6/26/2000 i.lOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.16E-16 9.00E-13 2.25E-13_ 5.07E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/26/2000 l.OOE-16 ~.OOE-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.31E-15 6.00E-13 1.50E-13 Not Analyzed !'Jot Applicable Not Applicable 12/26/2000 il..26E-16 9.00E-14 2.25E-14 l.OOE-16 Z.OOE-14 5.00E-15 .l.OOE-16 9.00E-13 2.25E-13 9.45E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable ., Not Applicable 3/26/2001 il.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.95E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable !'Jot Applicable 7/2/2001 l.OOE-16 . 9.00E~14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E·13· 6.56E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not ApRiicable 9/24/2001 il.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.16E-15 6.00E-13 1.50E-13 Not Analyzed Not A!JPiicable !'lot Aj)plicable 12/31/2001 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 2.20E-15 6.00E-13 1.50E-13 Not Analyzed Not A!J.plicable Not Applicable 4/1/2002 ;l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 .l.OOE-16 9.00E-13 2.25E-13 9.95E-15 6.00E-13 1.SOE-13 Not Analyzed Not Applicable Not Applicable 7/1/2002 ,1.25E-16 '9.00E-14 2.25E-14 1.43E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.25E-15 6.00E-13 1.50E-13 Not Analyzed Not A!Jplicable Not Applicable 9/30/2002 :LOOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 ,l.OOE-16 9.00E-13 2.25E-13 3.69E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/30/2002 il.OOE-16 fl.OOE-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.91E-15 6.00E-13 1,50E-13 Not Analyzed Not Applicable Not Applicable 3/31/2003 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 Z.OOE-14 5.00E-15 .l.OOE-16 9.00E-13 2.25E-13 6.16E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2003 ;I.OOE-16 9.00E-14 2.25E-14 l.OOE-16 Z.OOE-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 5.27E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/29/2003 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.23E-15 6.00E-13 1.50E-13 Not Analyzed Not A1Jplicable Not Applicable 12/29/2003 !I..OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 7.80E-15 6.00E-13 1.50E-13 !'lot Analyzed Not Applicable Not Applicable 3/29/2004 ,l,OOE-16 9.00E-14 2.25E-14 l.OOE-16 2,00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 2.04E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not ApP._Iicable 6/27/2004 ,l.OOE-16 9.00E-14 2.25E-14 .l.OOE-16 2.00E-14 5,00E-15 .l.OOE-16 9.00E-13 2.25E-13 3.09E-15 6.00E-13 1.SOE-13 Not Analyzed Not Applicable Not Applicable 9/27/2004 :LOOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 1.73E-14 6.00E-13 1,50E-13 i'Jot Analyzed Not Applicable Not Applicable 12/27/2004 l.OOE-16 -9.00E-14 2.25E-14-l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.30E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable_ Not Applicable 3/28/2005 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.88E-15 6.00E-13 1.50E-13 Not Analyzed Not Am>licable ,Not Applicable 6/29/2005 'l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13' 8.85E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/26/2005 ,l.OOE-16 9.00E-14 2.25E-14 1.99E-16 2.00E-14 5.00E-15 1.44E-16 9.00E-13 :Z.25E-13 3.81E-14 6.00E-13 1.50E-13 i'Jot Analyzed Not Applicable Not Applicable 1/3/2006 1.29E-16 9.00E-14 2.25E-14 l.OOE-16 .Z,OOE-14 5.00E-15 4.08E-16 9.00E-13 2.25E-13' 6.58E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable Date Effluent 9E-14 uCi/ml BHV-2U Effluent 2E-14 uCi/ml BHV-2T230 Effluent 9E-15 uCi/ml BHV-2R Effluent 6E-13 uCi/ml BHV-2PB Effluent 4e-15 uCi/ml BHV-2T232 Concentration Concentration Concentration Concentration Concentration Limit= limit= Limit= Limit= limit= ALARAGoal = " 2.2SE·14 uCi/ml ALARA Goal= SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARA Goal= l.SE-13 uCi/ml ALARAGoal = 1E-15 uCi/ml Pre 1994 MPC SE-12 uCi/ml Pre 1994 MPC BE-14 uCi/ml Pre 1994 MPC 2E-12 uCi/ml pre 1994 MPC 4E-12 uCi/ml pre 1994 MPC Not Applicable Limit= limit= Limit= Limit= limit= Pre 1994 ALARA 1.25E-12 uCi/ml Pre 1994 SE-13 uCi/ml Pre 1994 1E-12 uCi/ml Pre 1994 Not Applicable GOAL= ALARAGOAL= ALARAGOAL= ALARAGOAL= Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 'Cone EFC EFCA 4/3/2006 1.02E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.08E-14 6,00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/3/2006 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.10E·14 6.00E-13 1.SOE-13 Not Analyzed Not Applicable -Not Applicable 10/2/2006 1.30E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.68E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 1/1/2007 1.24E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.38E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/2/2007 1.40E-16 g.OOE-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.63E-14 6.00E-13 1.50E-13 f'lot Analyzed Not Applicable Not Applicable 7/2/2007 1.04E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.36E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Apjjlicable 9/30/2007 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.24E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/31/2007 ~.91E-16 '9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 'l..OOE-16 9.00E-13 2.25E-13 1.18E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/30/2008 l..OOE-16 9.00E-14 2.25E-14 l..OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.49E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2008 1..29E-16 19.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E·13 2.25E·13 4.82E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/30/2008 2.73E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l..OOE-16 9.00E-13 2.25E-13 8.30E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable NotApplicable 12/31/2008 5.71E-16 9.00E-14 2.25E-14 1..61E-16 2.00E-14 5.00E-15 1.25E-16 9.00E-13 2.25E-13 2.04E-14 6.00E-13 1.50E-13 Not Analyzed Not AQplicable Not Applicable 3/15/2009 3.96E-16 9.00E-14 2.25E-14 1.38E-16 2.00E-14 5.00E-15 1.07E-16 9.00E-13 2.25E-13 4.81E-15 6.00E-13 1.50E-13 Not Analyzed . Not Applicable Not Applicable 6/15/2009 1..24E-17 9.00E-14 2.25E-14 4.64E-17 2.00E-14 S.OOE-15 5.11E-17 9.00E-13 2.25E-13 4.58E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/15/2009 2.43E-16 9.00E-14 2.25E-14 5.28E-17 2.00E-14 S.OOE-15 4.84E-17 9.00E-13 2.25E-13 1.19E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/15/2009 5.72E-16 9.00E-14 2.25E-14 2.94E-17 2.00E-14 .S.OOE-15 2.57E-17 9.00E-13 2.25E-13 6.70E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/31/2010 5.47E-16 S.OOE-14 2.25E-14 1.42E-17 2.00E-14 S.OOE-15 4.66E-17 '9.00E-13 2.25E-13 8.24E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2010 3.58E-16 9.00E-14 2.25E-14 6.64E-17 2.00E-14 S.OOE-15 9.90E-17 9.00E-13 2.25E-13 2.01E-15 6.00E-13 1.50E-13 'Not Analyzed Not Applicable ' ·Not Applicable 9/30/2010 ~.91E-16 "9.00E-14 2.25E-14 4.48E-17 2,00E-14 5.00E-15 5.72E-17 9,00E-13 2,2SE-13 1.08E-15 6,00E-13 1.50E-13 Not Analyzed Not Applicable Not ApQiicable 12/31/2010 5.73E-16 9.00E-14 2.25E-14 7.24E-17 2.00E-14 S.OOE-15 6.76E-17 9.00E-13 2.25E-13 1.35E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/4/2011 3.79E-16 9.00E-14 2.25E-14 4.01E-17 2.00E-14 S.OOE-15 9.11E-17 9.00E-13 2.25E-13 1.06E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/4/2011 3.07E-16 9.00E-14 2.25E-14 8.54E-17 2.00E-14 S.OOE-15 9.21E-17 ~ 9.00E-13 2.25E-13 7.21E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 10/3/2011 1.17E-16 9.00E-14 ,2.25E-14 3.04E-17 2.00E-14 S.OOE-15 2.81E-17 9.00E-13 2.25E-13 1.03E-14 6.00E-13 1.50E-13 Not AnaJyzed Not Applicable Not Applicable 1/3/2012 3.65E-16 9.00E-14 2.25E-14 2.72E-17 2.00E-14 S.OOE-15 4.54E-17 9.00E-13 2.25E-13 1.58E-14 6.00E-13 1.50E-13 Not Analyzed · Not Applicable Not Applicable 4/3/2012 4.22E-16 9.00E-14 ;2.25E-14 1.15E-16 2.00E-14 S,OOE-15 2.77E-16 9.00E-13 2.25E-13 1.58E-14 6,00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/2/2012 ~.39E-16 9.00E-14 2.25E-14_ 1.56E-16 2.00E-14 5.00E-15 1.74E-16 g.OOE-13 2.25E-13 8.60E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 10/1/2012 3.13E-16 9.00E-14 2.25E-14 4.13E-17 2.00E-14 S.OOE-15 3.04E-17 g.OOE-13 2.25E-13 1.03E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/31/2012 2.76E-16 9.00E-14 ,2.25E-14 5.41E-17 2.00E-14 S.OOE-15 7,05E-17 9.00E·13 2.25E-13 1.48E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable -3/25/2013 3.38E-16 9.00E-14 2.25E-14 3.94E-17 2.00E-14 S.OOE-15 8.32E-17 9.00E-13 2.25E-13 L42E-14 6.00E-13 L50E-13 Not Analyzed Not Applicable Not Applicable 7/2/2013 4,06E-16 9.00E-14 2.25E-14 4.89E-17 2.00E-14 5.00E-15 8.06E-17 9.00E-13 2.25E·13 4.93E-15 6.00E-13 L50E-13 Not Analyzed Not Apl'llicable Not Applicable 9/30/2013 1.76E-16 iJ.OOE-14 2.25E-14-2.52E-17 2.00E-14 5.00E-15 6.13E-17 9.00E-13 2.25E-13 4.90E-15 6.00E-13 LSOE-13 Not Analyzed -Not Applicable Not Applicable 12/30/2013 6,20E-16 9.00E-14 2.25E-14 4,19E-17 2.00E-14 S.OOE-15 3.72E-17 9.00E-13 2.25E-13 2.50E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/31/2014 4.63E-16 9.00E-14 2.25E-14 4.97E-17 2.00E-14 S.OOE-15 1.15E-16 9.00E-13 2.25E-13 1.49E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2014 3.04E-16 9.00E-14 'z.25E-14. 7.92E-17 2.00E-14 S.OOE-15 L82E-16 9.00E-13 2.25E-13 1.21E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/30/2014 4.89E-16 9.00E-14 2.25E-14 6.01E-17 2.00E-14 S.OOE-15 4.47E-17 9.00E-13 2.25E-13 1.10E-14 6.00E-13 1.50E-13 9.35E-18 4.00E-15 1.00E-15 12/29/2014 l.OOE-16 9.00E-14 2.25E-14 4.00E-17 2.00E-14 S.OOE-15 3.00E-17 9.00E-13 2.25E-13 2.20E-14 6.00E-13 1.50E-13 4.00E-18 4.00E-15 l.OOE-15 3/30/2015 5.00E-16 9.00E-14 2.25E-14 2,00E-17 2.00E-14 S.OOE-15 3.00E-17 9.00E-13 2.25E-13 2.30E-14 6.00E-13 1.50E-13 4,00E-18 4.00E-15 l.OOE-15 6/29/2015 LOOE-16 9.00E-14 2.25E-14 4.00E-17 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.40E-14 6.00E-13 1.50E-13 8.00E·18 4.00E-15 l.OOE-15 9/28/2015 5.00E-16 9.00E-14 2.25E-14 9.00E-17 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.00E-14 6.00E-13 1.50E-13 6.00E-18 4.00E-15 l.OOE-15 12/28/2015 l.OOE-16 9.00E-14 ·2.25E-14 S.OOE-17 2.00E-14 5.00E-15 3.00E-16 9.00E-13 2.25E-13 2.20E-14 6.00E-13 1.50E-13 3.00E-18 4.00E-15 l.OOE-15 3/28/2016 7.00E-16 9.00E-14 2.25E-14 6.00E-18 2.00E-14 5.00E-15 S.OOE-17 9.00E-13 2.25E-13 1.50E-14 6.00E-13 1.SOE-13 4.00E-18 4.00E-15 1.00E-15 6/27/2016 2.00E-16 9.00E-14 '2.25E-14 3.00E-17 2.00E-14 5.00E-15 3.00E-16 9.00E-13 2.25E-13 1.30E-14 6.00E-13 1.50E-13 4.00E-18 4.00E-15 1.00E-15 9/27/2016 4.20E-16 9.00E-14 i.25E-14 6.90E-17 2.00E-14 S.OOE-15 8.10E-17 9.00E-13 2.25E-13 l.OOE-14 6.00E-13 1.50E-13 5.20E-17 4.00E-15 1.00E-15 12/27/2016 4.10E-16 9.00E-14 2.25E-14 1.90E-17 2.00E-14 5.00E-15 5.00E·17 9.00E-13 2.25E-13 2.10E-14 6.00E-13 1.50E-13 2,20E-18 4.00E-15 l.OOE-15 -- ...... ...... ...... 0 0 0 0 0 0 m m m I I I ...... ...... ...... 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C! - - - - - - I'-..-I w 0 C! ..- g~-das 9~-das 17~-das 8~-das c~-das ~ ~-das o~-das 6o-das so-das Lo-das go-d as so-das 17o-das 8o-das co-das w-das oo-das 66-das 95-das L6-das 95-das 95-das 175-das 86-das c6·das ~6-das 06-das 6s-das ss-das Ls-das gg-das gg-das 179-das 8s-das cs-das ~s-das - 0 c 0 ; m .... -c C1) (.) c 0 0 C\1 ('I) C\1 I E :I "i: 0 ..c I- N > J: III e :::. (.) :I It) ,.... I UJ '<!" 11 - :!:: E .§ [) ...J :I I: It) o ,.... ·-I ~~ -. 1:'1"'" ~ II 5iii (.)~ 'E ct Gl a: .::!<~: =:...J UJ <I: 0 ,.... 0 0 + uJ UJ 0 0 ~ ~ ,.... (\J C') ""' l.{) co 1'-0 0 0 0 0 0 uJ I I uJ uJ I UJ UJ UJ 0 0 0 0 0 0 ~ ~ ~ ~ ~ ~ ,.... ,.... co 0) 0 (\J C') ""' 0 0 ,.... ,.... ,.... ,.... I uJ uJ I I I I UJ UJ UJ UJ UJ 0 0 0 0 0 0 0 0 0 0 ~ ~ ~ ~ i81eos Bo,j ,.... IJ 1\ l.{) co 1'-,.... ,.... ,.... I I I UJ UJ UJ 0 0 0 ~ ~ ~ co uJ 0 ~ 9~-oaa 9 ~-/\ON 9~-PO 9~-das 9 ~-Bnv 9~-1nr 9~-unr 9 ~ -ABV\J 9 ~ -JdV 9 ~ -JBV\J 9 ~-qa.:J 9~-uer 9~-oaa 9 ~-/\ON 9~-PO 9~-das 9 ~-Bnv 9~-unr 9 ~ -ABV\J 9 ~ -JdV 9 ~ -JBV\J 9 ~-uer v~-oaa V ~-/\ON TAB3 BHV-3 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent SE-14 uCi/ml BHV-3U Effluent ZE-14 uCi/ml BHV-3TZ30 Effluent 9E-13 uCi/ml BHV-3R Effluent 6E-13 uCi/ml BHV-3PB Concentration Concentration Concentration Concentration Limit= Limit= Limit= limit= ALARAGoal = 2.25E-14 uCi/ml ALARA Goal= SE-15 uCi/ml ALARAGoal= Z.ZSE-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml Pre 1994 MPC SE-12 uCi/ml Pre 1994 MPC BE-14 uCi/ml Pre 1994 MPC ZE-12 uCi/ml Pre 1994 MPC 4E-12 uCi/ml Limit= limit= Limit= Limit= Pre 1994 ALARA l.ZSE-12 uCi/ml Pre 1994 ALARA se-u ucirm1 Pre 1994 ALARA 1E-1Z uCi/ml GOAL= GOAL= GOAL= Cone EFC EFCA Cone EFC EFCA Cone EFC , EFCA Cone EFC EFCA 9/28/1981 1.74E-15 S.OOE-12 1.2SE-12 9.02E-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 S.OOE-13 1.54E-14 4.00E-12 l.OOE-12 12/14/1981 1.59E-15 S.OOE-12 psE-12 5.03E-16 8.00E-14 2.00E-14 1.30E-16 2.00E-12 S.OOE-13 2.25E-14 4.00E-12 l.OOE-12 I 3/29/1982 3.76E-16 S.OOE-12 1.25E-12 5,25E-16 8.00E-14 2.00E-14 4.08E-16 2.00E-12 S.OOE-13 1.96E-14 4.00E-12 l.OOE-12 6/30/1982 3.83E-16 5.00E-12 1.25E-12 2.16E-16 8.00E-14 2.00E-14 1.41E-15 2.00E-12 I S.OOE-13 2.40E-14 4,00E-12 l.OOE-12 9/27/1982 5.95E-16 5.00E-12 1.25E-12 1.44E-15 8.00E-14 2.00E-14 5.36E-16 2.00E-12 S.OOE-13 1.43E-14 4.00E-12 i.OOE-12 1/3/1983 z.OSE-16 S.OOE-12 1.25E-12' 1.23E-16 8.00E-14 2.00E-14 l.lOE-16 2.00E-12 S.OOE-13 3,01E-14 4.00E-12 l,OOE-12 4/4/1983 1.00E-16 S.OOE-12 1.25E-12 6.94E-17 8.00E-14 2.00E-14 6.11E-17 2.00E-12 5.00E-13 1.39E-14 4.00E-12 l.OOE-12 6/30/1983 3.06E-16 S.OOE-12 1.25E-12 9.59E-17 8.00E-14 2,00E-14 2.08E-16 ,2.00E-12 S.OOE-13 1.70E-14 4.00E-12 l.OOE-12 10/3/1983 1.91E-16 5.00E-12 1.25E-12_ 3.05E-16 8.00E-14 2.00E-14 2.79E-16 2.00E-12 5.00E-13 1.76E-14 4.00E-12 l.OOE-12 1/3/1984 3.01E-16 5.00E-12 1.25E-12 9.51E-17 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 S.OOE-13 9.17E-15 4,00E-12 l.OOE-12 4/2/1984 8.22E-16 , 5.00E-12 1.25E-12 7.52E-16 8.00E-14 2.00E-14 5.20E-17 2.00E-12 5.00E-13 3.47E-14 4.00E-12 l.OOE-12 7/2/1984 5.29E-16 5.00E-12 l .25E-12 6.18E-16 8,00E-14 2,00E-14 1.40E-16 :z.OOE-12 5.00E-13 1.32E-14 4.00E-12 l.OOE-12 10/1/1984 1.74E-16 5.00E-12 :1.25E-12 7.10E-17 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 S.OOE-13 1.08E-14 4.00E-12 l.OOE-12 1/2/1985 l.OOE-17 5.00E-12 ,1.25E-12 7.10E-17 S,OOE-14 2.00E-14 7.80E-17 2.00E-12 S.OOE-13 2.73E-14 4.00E-12 l.OOE-12 4/1/1985 l.OOE-16 5.00E-12 1.25E-12 2. 76E-16 8.00E-14 2.00E-14 4.10E-17 2.00E-12 S.OOE-13 1.12E-14 4.00E-12 l.OOE-12 7/1/1985 1.04E-16 5.00E-12 1.25E-12 l.OOE-16 S.OOE-14 2.00E-14 1.00E-16 2.00E-12 . S.OOE-13 1.64E-14 4.00E-12 l.OOE-12 9/30/1985 1.00E-16 S.OOE-12 1.25E-12 l.OOE-15 8.00E-14 2.00E-14 l.OOE-16 l.OOE-12 5.00E-13 1,73E-14 4.00E-12 l.OOE-12 1/2/1986 1.03E-15 5.00E-12 1.25E-12 3.17E-16 S.OOE-14 2.00E-14 1.25E-16 :Z.OOE-12 5.00E-13 1.21E-17 4.00E-12 l.OOE-12 4/1/1986 8.04E-16 5.0QEC12 1.25E-12 1.93E-17 8.00E-14 2.00E-14 1.54E-16 2.00E-12 S.OOE-13 1.69E-14 4.00E-12 l.OOE-12 6/30/1986 4.29E-16 5.00E-12 1.25E-12 1.77E-16 B.OOE-14 2.00E-14 2.83E-16 e,OOE-12 S.OOE-13 1.97E-14 4.00E-12 l.OOE-12 10/27/1986 6.45E-16 5.00E-12 1.25E-12 9.89E-17 B.OOE-14 2.00E-14 4.16E-15 2.00E-12 5.00E-13 1.64E-14 4.00E-12 l.OOE-12 12/15/1986 1.31E-16 -5.00E-12 1.25E-12 O.OOE+OO B.OOE-14 2.00E-14 4.16E-17 2.00E-12 5.00E-13 4.60E-15 4.00E-12 l.OOE-12 3/16/1987 2.01E-16 5.00E-12 1.25E-12 1.20E-16 8.00E-14 2.00E-14 5.73E-17 2.00E-12 5.00E-13 1.60E-14 4.00E-12 l.OOE-12 5/11/1987 2.16E-16 S.OOE-12 1.25E-12 1.96E-16 s.OOE-14 2.00E-14 7.38E-17 2.00E-12 5.00E-13 1.59E-14 4.00E-12 l.OOE-12 9/9/1987 2.41E-16 S.OOE-12 1.25E-12 2.18E-16 8.00E-14 2.00E-14 3.52E-17 2.00E-12 S.OOE-13 1.46E-14 4.00E-12 l.OOE-12 11/2/1987 2.44E-16 5.00E-12 1.25E-12 2,32E-16 8.00E-14 2.00E-14 2.37E-17 2.00E-12 5.00E-13 2.48E-14 4.00E-12 l.OOE-12 2/16/1988 8.08E-16 S.OOE-12 p5E-12 2.55E-16 8.00E-14 2.00E-14 3.42E-16 2.00E-12 S.OOE-13 5.61E-14 4.00E-12 l.OOE-12 5/18/1988 1.14E-16 S.OOE-12 1.25E-12 4.14E-17 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 5.00E-13 1.20E-14 4.00E-12 1.00E-12 8/15/1988 2.08E-16 S.OOE-12 1.25E-12 3.06E-16 8.00E-14 2.00E-14 3.65E-17 2.00E-12 5.00E-13 1.36E-14 4.00E-12 l.OOE-12 11/14/1988 4.21E-16 S.OOE-12 1.25E-12 2.93E-16 8.00E-14 2.00E-14 1.09E-16 2.00E-12 5.00E-13 2.48E-14 4.00E-12 l.OOE-12 2/13/1989 4.45E-16 S.OOE-12 1.25E-12 4.78E-17 8.00E-14 2.00E-14 2.47E-17 2.00E-12 5.00E-13 3.34E-14 4.00E-12 1.00E-12 5/15/1989 1.05E-16 S.OOE-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 2.45E-17 2.00E-12 5.00E-13 6.56E-15 4.00E-12 1.00E-12 8/14/1989 1.31_E-~6 S.OOE-12 1.25E-12 5.85E-17 8.00E-14 2.00E-14 3.97E-17 2.00E-12 5.00E-13 6.75E-15 4.00E-12 1.00E-12 11/13/1989 1.67E-16 , S.OOE-12 ,1.25E-12 3.87E-17 8.00E-14 2.00E-14 8.03E-17 2.00E-12 S.OOE-13 1.69E-14 4.00E-12 l.OOE-12 2/12/1990 4.43E-16 S.OOE-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 3.50E-17 2.00E-12 5.00E-13 2.37E-14 4.00E-12 1.00E-12 5/14/1990 3.84E-16 S.OOE-12 1.25E-12 2.54E-16 S.OOE-14 2.00E-14 1.02E-16 2.00E-12 5.00E-13 1.68E-14 4.00E·12 1.00E-12 8/13/1990 7.27E-17 S.OOE-12 1.25E-12 2.87E-16 8.00E-14 2.00E-14 1.21E-17 2.00E-12 5.00E-13 7.86E-15 4.00E-12 l.OOE-12 11/12/1990 1.84E-16 -~ S.OOE-12 :1.25E·12· 1.34E-16 8.00E-14 2.00E-14 8.53E-17 2.00E·12 5.00E-13 2.01E-14 4.00E-12 l.OOE-12 2/11/1991 4.66E-17 :S,.OOE-12 1.25E-12 8.48E-16 8.00E-14 2.00E-14 1.94E-17 2.00E-12 5.00E·13 3.69E-14 4.00E·12 1.00E·12 5}13/1991 5.05E·17 . S.OOE-12 '1.25E-12 7.40E·17 8.00E·14 2.00E-14 7.00E-18 2.00E·12 5.00E-13 1.50E-14 4.00E-12 l.OOE-12 8/12/1991 7.14E-17 'S.OOE-12 "1.25E-12. 6.22E-17 8.00E-14 2.00E-14 7.95E-17 2.00E-12 5.00E-13 1.77E-14 4.00E-12 l.OOE-12 11/11/1991 1.41E-17 ~.OOE-12 1.25E-12 2.19E-18 8.00E·14 2.00E-14 2.75E·17 2.00E-12 5.00E·13 1.18E-14 4.00E-12 l.OOE-12 2/10/1992 8.12E-17 I .S.OOE-12 1,25E-12, 2.35E-17 S.OOE-14 2.00E-14 2.76E-18 2.00E-12 5.00E·13 3.57E-14 4.00E·12 1.00E-12 5/11/1992 9.18E-17 S.OOE-12 1.25E-12 5.80E-17 S.OOE-14 2.00E-14 3.36E-17 2.00E-12 5.00E-13 1.28E·14 4.00E-12 l.OOE-12 8/10/1992 2.00E-18 S.OOE-12 1.25E-12 4.19E-17 S.OOE-14 2.00E-14 Z.OOE-18 2.00E-12 5.00E-13 1.59E-14 4.00E-12 1.00E-12 11/9/1992 4.00E·17 S.OOE-12 1.25E-12 2.68E·17 S.OOE-14 2.00E-14 1.07E-17 Z.OOE-12 5.00E-13 1.81E-14 4.00E·12 1.00E-12 2/9/1993 7.94E-17 I .S.OOE-12 1.25E·12 l.OOE-16 S.OOE-14 2.00E-14 1.09E-16 Z.OOE-12 5.00E-13 2.69E-14 4.00E-12 1.00E-12 5/10/1993 1.60E-17 S.OOE-12 1.25E-12 5,07E-17 S.OOE-14 2,00E-14 7.64E-17 2.00E-12 ·5.00E-13 1.26E-14 4.00E-12 l.OOE-12 8/10/1993 6.00E·17 .S.OOE-12 1.25E-12 6,00E-18 S.OOE-14 2.00E-14 1,00E-16 2.00E-12 5.00E·13 1.50E·14 4.00E-12 l.OOE-12 Date Effluent 9E-14 uCi/ml BHV-3U Effluent ;zE-14 uCi/ml BHV-3T230 Effluent 9E-13 uCi/ml BHV-3R Effluent 6E-13 uCi/ml BHV-3PB Concentration Concentration Concentration Concentration Limit= Limit= Limit= limit= ALARAGoal = 2.25E-14 uCi/ml ALARA Goal= SE-15 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml Pre 1994 MPC SE-12 uCi/ml Pre 1994 MPC SE-14 uCi/ml Pre 1994 MPC 2E-12 uCi/ml Pre 1994 MPC 4E-12 uCi/ml Limit= Limit= Limit= Limit= Pre 1994 ALARA 1.25E-12 u<;i/ml Pre 1994 A LARA SE-13 uCi/ml Pre 1994 ALARA 1E-12 uCi/ml GOAL= GOAL= GOAL= Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 11/8/1993 1.00E-16 5.00E-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 5.00E-13 2.10E-14 4.00E-12 l.OOE-12 2/7/1994 1.61E-16 ;i.OOE-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 2.22E-16 2.00E-12 5.00E-13 2.23E-14 4.00E-12 l.OOE-12 5/9/1994 2.77E·16 5.00E·12 1.25E·12 2.80E·17 8.00E·14 2.00E-14 8.37E-18 2.00E-12 5.00E-13 1.40E-14 4.00E-12 l.OOE-12 8/9/1994 7.39E-17 :5.00E-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 1.14E-16 ~ 2.00E-12 5.00E-13 l.OOE-16 4.00E-12 l.OOE-12 11/7/1994 9.05E-17 5.00E-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-13 l.OOE-16 4.00E-12 l.OOE-12 2/7/1995 7.99E-17 9.00E-14 ' 2.25E-14 9.60E-17 2.00E-14 S.OOE-15 9.60E-17 9.00E-13 2.25E-13 9.05E-15 6.00E-13 1.50E-13 5/9/1995 9.40E-17 9.00E-14 2.25E-14 9.80E-17 2.00E-14 S.OOE-15 8.60E-17 9.00E-13 2.25E-13 2.88E-15 6.00E-13 1.50E-13 8/9/1995 i7.30E-17 9.00E-14 2.25E-14 9.20E-17 2.00E-14 S.OOE-15 4.40E-17 9.00E-13 2.25E-13 1.96E-15 6.00E-13 1.50E-13 11/11/1995 '3,16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 S,OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 2/5/1996 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 5/6/1996 L31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 8/5/1996 a.OOE-16 9.00E-14 2.25E-14 3.43E-16 2,00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 11/6/1996 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 ~ 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 2/6/1997 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 5/5/1997 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 L53E-14 6.00E-13 1.50E-13 8/11/1997 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 1/5/1998 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 L91E-14 6,00E-13 1.50E-13 4/28/1998 ;!.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/31/1998 :J..31E-16 9.00E-14 2,25E-14 1.39E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/28/1998 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/28/1998 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2,00E-14 S.OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/29/1999 3.41E-16 ~.OOE-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/3/1999 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 L53E-14 6.00E-13 1.50E-13 9/27/1999 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/28/1999 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 S.OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/28/2000 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 Ll..18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/26/2000 P1E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S.OOE-15 l.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/26/2000 p.OOE-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/26/2000 9.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 .9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/26/2001 3.41E-16 ~.OOE-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 l.lSE-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/2/2001 i.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/24/2001 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/31/2001 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 S.OOE-15 6.58E-17 9.00E-13 2.25E-13 L91E-14 6.00E-13 1.50E-13 4/1/2002 B.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2,69E-14 6.00E-13 1.50E-13 7/1/2002 :t.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 L53E-14 6,00E-13 1.50E-13 9/30/2002 3.00E-16 ~.OOE-14 2.25E-14 3.43E-16 2,00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/30/2002 !3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6,00E-13 1.50E-13 3/31/2003 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 . 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/30/2003 '1.31E-16 9.00E-14 2.25E-14 1.39E-16 2,00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6,00E-13 1.50E-13 9/29/2003 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/29/2003 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 S.OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 l.SOE-13 3/29/2004 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9,00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/27/2004 iJ..31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S,OOE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/27/2004 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/27/2004 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 S.OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/28/2005 3.41E-16 9.00E-14 2,25E-14 2.26E-16 2,00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/29/2005 11.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 l.SOE-13 9/26/2005 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6,00E-13 1.50E-13 1/3/2006 ~.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E·13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 Date Effluent 9E-14 uCi/ml ~HV-3U Effluent 2E-14 uCi/ml BHV-3T230 Effluent 9E-13 uCi/ml BHV-3R Effluent 6E-13 uCi/ml BHV-3PB Concentration Concentration Concentration Concentration Limit= Limit= Limit= Limit= AlARAGoal = 2.25E-14 uCi/ml ALARAGoal = SE-15 uCi/ml ALARA Goal= 2.25E-l3 uCi/ml ALARA Goal= 1.5E-13 uCi/ml Pre 1994 MPC SE-12 uCi/ml Pre 1994 MPC BE-14 uCi/ml Pre 1994 MPC 2E-12 uCi/ml Pre 1994 MPC 4E-12 uCi/ml Limit= Limit= Limit= Limit= Pre 1994 AlARA 1.25E-12 uCi/ml Pre 1994 A LARA SE-13 uCi/ml Pre 1994 AlARA 1E-12 uCi/ml GOAL= GOAL= GOAL= Cone EFC ~ EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 4/3/2006 3.41E-16 ~.OOE-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 l.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/3/2006 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E·13 1.50E-13 10/2/2006 3.00E-16 9.00E·14 2.25E-14 3.43E-16 2.00E·14 5.00E-15 3.99E·16 9.00E·13 2.25E-13 1.31E-14 6.00E·13 1.50E·13 1/1/2006 3.16E-16 S.OOE-14 • 2.25E·14 1.31E-16 2.00E-14 5.00E·15 6.58E-17 9.00E·13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 4/2/2007 3.41E-16 9.00E-14 2.25E·14 2.26E-16 2.00E-14 5.00E·15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/2/2007 l.31E·16 9.00E-14 2.25E·14 1.39E·16 2.00E·14 S.OOE-15 1.82E-16 9.00E·13 2.25E·13 1.53E-14 6.00E·13 1.50E·13 9/30/2007 3.00E-16 9.00E·14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/31/2007 '3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 S.OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/31/2008 i3.41E-16 ~.OOE-14 2.25E-14 2.26E-16 2.00E-14 S.OOE-15 l.18E-16 9.00E-13 i.25E·l3 2.69E-14 6.00E·l3 1.50E-13 6/30/2008 p1E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S.OOE-15 l.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/30/2008 B.OOE-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3 99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/31/2008 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 fi.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/15/2009 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 S.OOE-15 j;l.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/15/2009 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 :LB2E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/15/2009 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/15/2009 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 G.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/31/2010 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E'13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/30/2010 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/30/2010 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 "2.25E-13 l.31E-14 6.00E-13 1.50E-13 12/31/2010 ~.16E-16 9.00E-14 2.25E-14 :1.31E·16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 4/4/2011 3.41E-16 9.00E-14 2.25E-14 2,26E-16 2.00E-14 S.OOE-15 l.lBE-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/4/2011 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E·13· 1.53E-14 6.00E-13 1.50E-13 10/3/2011 p.OOE-16 9.00E-14 2.25E-14 B.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 l.SOE-13 1/3/2012 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 S.OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 4/3/2012 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/2/2012 1.31E-16 9.00E-14 ·2.25E-14 1.39E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 10/1/2012 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/31/2012 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6,58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/25/2013 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E·13· 2.69E-14 6.00E-13 1.50E-13 7/2/2013 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/30/2013 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/30/2013 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/31/2014 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 l.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/30/2014 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/30/2014 3,00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 ,2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/29/2014 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9,00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3}30}2015 }.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/29/2015 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 '2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/28/2015 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 !l.OOE-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/28/2015 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/28/2016 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/27/2016 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/27/2016 .3,00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 !J.OOE-13 2.25E-13 1.31E-14 6.00E-13 l.SOE-13 12/27/2016 3.16E-16 9.00E-14 !2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 (Log Scale) _. _. 0 0 0 0 0 0 0 0 m m m m I I I I _. _. _. ...... 00 ....... 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I' p. •• f: •=:::: ~ .~ .~ 5! .~ ~ .~ f: .~ ~ .~ ~ .~ ~ • p. l•f; ~ I• F. f::_ ~ r-r--.. I' r-. ~ .... ~ ~ .._... -.. ... F""' <0 ,..... I UJ 0 ~ ,..... p.~ • ... ~ I'-,.... Li.J 0 ~ ,..... - - - - co ,.... I UJ 0 ~ ,..... 9~-das 9~-das v~-das £~-das c::~-das ~ ~-das o~-das 60-das so-das Lo-das 9o-das 9o-das vo-das £o-das c::o-das ~o-das oo-das 66-das B6-das L6-das 96-das 96-das v6-das £6-das <::6-das ~6-das oe-das 6B-das ss-das LB-das 99-das 99-das vs-das £B-das c::s-das ~s-das 1/) c 0 +::: ca ... -c Cl) (J c 0 0 co C\1 C\1 I E ::::s '1J ca a: ('I) > J: m I ~ C\J ,.... ,.... I I w w 0 0 ~ ~ ~~ .., C') -.;t 1.0 ,.... ,.... w I I w w 0 0 0 ~ 0 0 ~are~s oo1f f-r--. F: ft-... I' ft-... :-~ F-~ f-~ t-~ F-~ F-~ i' ~ ~::: ~ ~ ~ F-~ f-~ F: ~ ~ ~ ;;., ~ ...... ~ ::;;;. ~ tel:::: ~ f', ~ ~ .. J..... 1---- """ ~ ~ ~ ~ ~ __. !::>+ c.o w 0 ~ ,.... tt ~tt It !II"" ' 1"-,.... I w 0 ~ ,.... - - - - - ' 00 w 0 ~ ,.... g~-das 9~-das 17~-das £~-das c~-das ~ ~-das o~-das 6o-das so-das La-das go-das so-das vo-das £o-das co-das ~o-das oo-das 66-das 96-das L6-das 96-das 96-das v6-das £6-das c6·das ~6-das 06-das 6s-das gg-das Ls-das gg-das ss-das vs-das £s-das cs-das ~s-das - w c 0 ... C'CS ... -c Cl) (,) c 0 0 0 T"" N I "C C'CS Cl) ...J C") > ::I: m uJ 0 ~ ..... ' C\J (t) ..... I uJ L.U 0 0 ~ 0 ..... ..... [tl: ~ It!: ~ [tl: [tl: ~ ~ [tl: ~ ~ ~ ~ It!: ~ ftc: ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ 1 .... ~ ~ leo Ito F:; ~ I• ~ ,. ~ ~ t-r+ tt ~ I~ ~ ,. ~ C¥ ~~ ~ I ~ • ...... '<:t uJ 0 0 (are~s oo1) ~ ' 10 ..... I L.U 0 ~ . (!) ..... I L.U 0 0 - - - I"-..... I L.U 0 ~ 9~-das g~-das v~-das 8~-das c::~-das ~ ~-das o~-das 6o-das eo-das Lo-das go-d as go-d as vo-das 8o-das c::o-das ~o-des oo-das 66-das B6-das L6-das 96-das 96-das v6-das 86-das <::6-das ~6-das 06-das 6B-das BB-das LB-das gg-das gg-das pg-das 8B-das c::e-das ~g-das TAB4 BHV-4 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent 9E-14 uCi/ml BHV-4U Effluent 2E-14 uCi/ml BHV-4T230 Effluent 9E-13 uCi/ml BHV-4R Effluent 6E-13 uCi/ml BHV-4PB Effluent 4e-15 uCi/ml BHV-4T232 Concentration Concentration Concentration Concentration Concentration Limit= Limit= Limit= Limit= Limit.,_ ALARAGoal-2.25E-14 uCi/ml ALARA Goal= 5E-15 uCi/ml ALARAGoal= 2.25E-13 uCi7ml ALARA Goal= 1.SE-13 uCi/ml ALARAGoal = 1E-15 uCi/ml Pre 1994 MPC SE-UuCi/ml Pre 1994 MPC BE-14 uCi/ml Pre 1994MPC 2E-12 uCi/ml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable Limit= Limit= Limit= Limit= Limit= Pre 1994 1.25E-12 uCi/ml Pre 1994 ALARA SE-13 uCi/ml Pre 1994 1E-12 uCi/ml Pre 1994 Not Applicable ALARAGOAL= GOAL= ALARAGOAL= ALARAGOAL= Cone . EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 5.20E-15 S.OOE-12 1.25E-12, 2.93E-15 8.00E-14 2.00E-14 2.74E-15 . 2.00E-12 S.OOE-13 1.84E-14 4.00E-12 l.OOE-12 Not Analyzed Not J\pplicable Not Applicable 12/14/1981 ~.53E-15 5.00E-12 1.25E-12 1.78E-15 B.OOE-14 2.00E-14 2.29E-15 Z.OOE-12 S.OOE-13 2.54E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 3/29/1982 l.06E-15 5.00E-12 1.25E-12 1.42E-14 8.00E-14 2.00E-14 1.07E-15 Z.OOE-12 ~.OOE-13 2.31E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 6/30/1982 6.03E-15 S.OOE-12 1.25E·12 1.57E-14 8.00E-14 Z.OOE-14 2.62E-15 Z.OOE-12 S.OOE-13 2.25E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 9/27/1982 1.26E-14 S.OOE-12 1.25E-12 7.58E-16 8.00E-14 2.00E-14 5.35E-15 Z.OOE-12 5.00E-13 2.68E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not 1\p_plicable -1/3/1983 11.33E-15 S.OOE-12 1.25E-12 6.52E-16 8.00E-14 2.00E-14 6.04E-16 2.00E-12 5.00E-13 2.57E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Ap_plicable 4/4/1983 1.25E-15 S.OOE-12 . 1.25E·12' 7.17E-16 8.00E-14 2.00E·14 6.76E-16 Z.OOE-12 5.00E-13 2.00E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 6/30/1983 3.73E-16 S.OOE-12 1.25E·12 9.43E-16 8.00E-14 2.00E-14 4.13E-16 2.00E-12 S.OOE-13 1.20E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 10/3/1983 2.54E-16 S.OOE-12 1.25E-12 1.51E-16 B.OOE-14 2,00E-14 2.65E-16 2.00E-12 S.OOE-13 2.50E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 1/3/1984 2.76E-15 S.OOE-12 1.25E-12. 1.60E-16 8.00E-14 2.00E-14 1.05E-16 2.00E-12 S.OOE-13 1.59E-16 4.00E-12 l.OOE-12 Not Analyzed Not Applical>le Not Applicable 4/2/1984 4.27E-16 S.OOE-12 1.25E-12 2.33E-16 8.00E-14 2.00E-14 6.28E-16 2.00E-12 S.OOE-13 3.67E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable !'lot Ap_plicable 7/2/1984 2.57E-15 S.OOE-12 1.25E-12 1.36E-16 8.00E-14 2.00E-14 1.11E-16 2.00E-12 5.00E-13 1.58E-14 4.00E-12 l.OOE-12 Not Analyzed !'Jot Applicable !'lot Applicable 10/1/1984 4.18E-16 S.OOE-12 1.25E-12 3.54E-16 8.00E-14 2,00E-14 1.10E-17 2.00E-12 S.OOE-13 9.83E-15 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Af!plicable 1/2/1985 5.30E-17 5.00E-12 1.25E-12 3.55E-17 B.OOE-14 2.00E·14 7.00E-18 2.00E-12 S.OOE-13 2.57E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable !'Jot Applicable 4/1/1985 1.00E-16 S.OOE-12 1.25E·12 6.00E-16 B.OOE-14 2.00E·14 4.35E-17 2.00E-12 S.OOE-13 5.02E-15 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 7/1/1985 9.36E-16 5.00E-12 1.25E-12 2.33E-16 8.00E-14 2.00E-14 2.36E-16 2.00E-12 S.OOE-13 ' 7,48E-15 4.00E-12 1.00E-12 Not Analyzed Not Applicable NOt A_pplicable 9/30/1985 1.46E-15 S.OOE-12 1.25E-12 7.69E-16 8.00E-14 2.00E-14 5.38E-16 ;woe-12 S.OOE-13 7.86E-15 4.00E-12 l.OOE-12 Not Analyzed NoV\IJ_plicable Not Applicable 1/2/1986 8.40E-15 S.OOE-12 1.25E-12 7.60E-16 8.00E-14 2.00E-14 2.99E-16 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 4/1/1986 S.79E-15 5.00E-12 1.25E-12 S.80E-16 8.00E-14 2.00E-14 1.34E-15 Z.OOE-12 S.OOE-13 1.33E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 6/30/1986 5.19E-15 5.00E-12 1.25E-12 7.83E-16 8.00E-14 2.00E-14 2.20E-15 2.00E-12 S.OOE-13 7.14E-16 4.00E-12 1.00E·12 Not Analyzed Not Applicable Not Applicable 10/27/1986 4.60E-15 5.00E-12 1.25E-12 4.67E-16 8.00E-14 Z.OOE-14 2.37E-15 2.00E-12 5.00E-13 1.13E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Af!plicable 12/15/1986 2.75E-15 S.OOE-12 1.25E-12 5.90E-16 8.00E-14 2.00E-14 9.39E-16 .l.OOE-12 5.00E-13 1.20E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 3/16/1987 4.64E-15 5.00E-12 1.25E-12 1.18E-15 8.00E-14 2.00E-14 4.97E-16 Z.OOE-12 S.OOE-13 5.89E-14 4,00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/11/1987 4.35E-15 S.OOE-12 1.25E-12 1.23E-14 8.00E-14 2.00E-14 ~.13E-15 2.00E-12 S.OOE-13 2.21E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 9/9/1987 6.39E-15 5.00E-12 ' 1.25E-12 1.50E-14 8.00E-14 2.00E-14 2.26E-15 2.00E-12 5.00E-13 1.57E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 11/2/1987 6.72E-15 S.OOE-12 1.25E-12 4.53E-16 8.00E-14 2.00E-14 2.20E-15 2.00E-12 S.OOE-13 2.55E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 2/16/1988 1.91E-15 S.OOE-12 1.25E-12 1.35E-14 8.00E-14 2.00E-14 4.42E-16 2.00E-12 5.00E-13 4.44E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/18/1988 1,78E-14 5.00E-12 1.25E-12 4.39E-14 8.00E-14 2.00E-14 4.92E-16 2.00E-12 5.00E-13 1.38E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/15/1988 7.56E-15 S.OOE-12 1.25E-12 3.31E-14 8.00E-14 2.00E-14 1.51E-15 2.00E-12 5.00E-13 1.97E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/14/1988 1.47E-14 S.OOE-12 1.25E-12 1.56E-15 8.00E-14 2.00E-14 2.57E-15 2.00E-12 5.00E-13 2.12E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 2/13/1989 2.47E-15 S.OOE-12 1.25E-12 3.14E-15 8.00E-14 2.00E-14 6.94E-16 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable ,Not Applicable 5/15/1989 2.50E-16 5.00E-12 1.25E-12 7.68E-15 S.OOE-14 2.00E-14 9.03E-16 2.00E-12 S.OOE-13 8.05E-15 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 8/14/1989 6.50E-15 ,S.OOE-12 1.25E-12 4.72E-15 S.OOE-14 2.00E-14 2.35E-15 2.00E-12 5.00E-13 9.95E-15 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/13/1989 9.63E-15 S.OOE-12 1.25E-12 4.05E-15 8.00E-14 2.00E·14 4.03E-15 2.00E-12 5.00E-13 1.99E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/12/1990 8.92E-15 S.OOE-12 1.25E-12 3.56E-15 S.OOE-14 2.00E-14 2.89E-15 2.00E-12 S.OOE-13 2.69E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/14/1990 8.90E-15 S.OOE-12 1.25E-12 3.58E-15 8.00E-14 2.00E-14 2.33E-15 2.00E-12 S.OOE-13 2.09E-14 4.00E-12 LOOE-12 Not Analyzed Not Applicable NOt Applicable 8/13/1990 1.92E-15 S.OOE-12 1.25E-12 1.87E-15 8.00E-14 2.00E-14 5.06E-16 2.00E-12 5.00E·13" 8.86E-15 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/12/1990 2.91E-15 fj.OOE-12 1.25E-12 2.2SE-17 8.00E-14 2.00E-14 1.08E-15 2.00E-12 5.00E-13 2.19E-14 4.00E-12 LOOE-12 Not Analyzed Not Applicable Not Applicable 2/11/1991 1.67E-16 S.OOE-12 1,25E-12 7.89E-16 8.00E-14 2.00E-14 6.38E-17 2.00E-12 S.OOE-13 4.19E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/13/1991 1.87E-16 5.00E-12 1,25E-12 2.61E-15 8.00E-14 2.00E-14 3.54E-16 2.00E-12 S.OOE-13 1.40E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/12/1991 4.85E-16 S.OOE-12 1.25E-12 4.38E-16 8.00E-14 2.00E-14 1.27E-16 2.00E-12 S.OOE-13 2.20E-14 4.00E-12 l.OOE-12 !'Jot Analyzed Not Applicable Not Applicable 11/11/1991 '1.77E-16 S.OOE-12 1.25E-12 1.46E-16 8.00E-14 2.00E-14 3.76E-17 2.00E-12 S.OOE-13 1.15E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/10/1992 J..83E-16 S.OOE-12 1.25E-12 1.95E-15 8.00E-14 Z.OOE-14 1.33E-16 2.00E-12 5.00E-13 3.35E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 5/11/1992 4.40E-16 S.OOE-12 1.25E·12 2.56E-16 8.00E-14 2.00E-14 4.04E-16 2.00E-12 S.OOE-13 1.41E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 8/10/1992 9.09E-17 S.OOE-12 1.25E-12 1.15E-16 8.00E-14 2.00E·14 4.50E-17 ,Z.OOE-12 S.OOE-13 1.57E-14 4.00E-12 LOOE-12 Not Analyzed Not Applicable Not Applicable 11/9/1992 2.07E-16 5.00E-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 3.62E-17 2.00E-12 5.00E-13 2.24E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/9/1993 1.73E-16 S.OOE-12 1.25E-12 2.76E-17 8.00E-14 Z.OOE-14 2.89E-17 2.00E-12 S.OOE-13 3.08E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable S/10/1993 2.70E-17 5.00E-12 1.25E-12 2.50E-17 8.00E-14 2.00E·14 8.74E-17 2.00E-12 5.00E-13 1.25E-14 4.00E-12 1.00E-12 Not Analyzed Not Apf!licable Not Applicable 8/10/1993 9.00E-17 S.OOE-12 1.25E-12 1.76E-16 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 5.00E-13 1.50E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/8/1993 1.00E-16 S.OOE-12 1.25E-12 l.OOE-16 8.00E-14 2.00E·14 6.00E-17 2.00E-12 5.00E-13 1.75E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable Date Effluent 9E-14 uCi/ml BHV-4U Effluent ZE-14 uCi/ml BHV-4TZ30 Effluent 9E-13 uCi/ml BHV-4R Effluent 6E-13 uCi/ml BHV-4PB Effluent 4e-15 uCiTml BHV-4U32 C.oncentration Concentration Concentration Concentration Concentration limit= Limit= Limit= Limit= limit= AlARAGoal= 2.25E-14 uCiTml ' A LARA Goal = I SE-15 uCi/ml ALARA Goal-. 2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml AlARAGoal = 1E-15 uCi/ml Pre 1994MPC SE-12 uCi/ml Pre 1994 MPC 8E-14 uCi/ml Pre 1994 MPC 2E-12 uCi{ml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable Limit= limit= !.;mit= limit= limit= Pre 1994 1.25E-12 uCt/ml pre 1994 ALARA SE-13 uCi/ml Pre 1994 lE-12 uCi/ml Pre 1994 Not Applicable ALARAGOAL= GOAL= ALARAGOAL= ALARAGOAL= Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1994 l.lOE-16 5.00E-12 1.25E-12 3.38E-16 8.00E-14 2.00E-14 2.21E-16 2.00E-12 _?.OOE-13 3,08E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/9/1994 3.80E-16 5.00E-12 1.25E-12 2.82E-16 8.00E-14 2.00E-14 3.46E-16 2.00E-12 5.00E-13 1.73E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/9/1994 3.85E-16 5.00E-12 1.25E-12 3.53E-16 S.OOE-14 2,00E-14 l.OOE-16 2.00E-12 5.00E-13 l.OOE-16 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not AP-Plicable 11/7/1994 6.21E-17 S.OOE-12 1.25E-12 9.70E-17 S.OOE-14 2.00E-14 1.96E-16 2.00E-12 5.00E-13 1.00E-16 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Al!l!!.icable 2/7/1995 3.70E-16 9.00E-14 2.25E-14 9.80E-17 2.00E-14 5.00E-15 9.70E-17 9.00E-13 2.15E-13 8.84E-15 6.00E-13 1.50E-13 Not Analyzed Not AJ1Piicable Not Applicable 5/9/1995 9.40E-17 9.00E-14 2.25E-14 2.86E-16 2.00E-14 5.00E-15 1.90E-16 9.00E-13 2.25E-13 2.90E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 8/9/1995 1.45E-16 S.OOE-14 2.25E-14 2.31E-15 2.00E-14 5.00E-15 7.10E-17 9.00E-13 2.25E-13 2.70E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 11/11/1995 1.~3E-14 9.00E-14 2.15E-14 5.70E-15 l.OOE-14 5.00E-15 2.61E-15 9.00E-13 2.25E-13 5.60E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 2/5/1996 1.19E-14 9.00E-14 2.25E-14 3.80E-16 2.00E-14 5.00E-15 6.10E-15 9.00E-13 2.25E-13 6.48E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 5/6/1996 4.55E-16 9.00E-14 2.25E-14 3.57E-15 2.00E-14 5.00E-15 2.84E-16 9.00E-13 2.25E-13 7.68E-15 6,00E-13 1.50E-13 Not Analyzed 'Not Applicable Not Applicable 8/5/1996 7.78E-16 9.00E-14 2.25E-14 3.51E-15 2.00E-14 S.OOE-15 1.69E-16 9.00E-13 2.25E-13 4.90E-15 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 11/6/1996 1.36E-15 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 4.21E-16 9.00E-13 2.25E-13 l.lOE-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 2/6/1997 l.OOE-16 9.00E-14 2.25E-14 1.40E-16 2.00E-14 5.00E-15 1.03E-16 !l.OOE-13 2.25E-13 6.76E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 5/5/1997 l.OOE-16 9.00E-14 2.25E-14 4.00E-16 2.00E-14 5.00E-15 2.24E-16 9.00E-13 2.25E-13 4.55E-15 6,00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 8/11/1997 4.74E-16 9.00E-14 2.25E-14 9.07E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.2SE-13 5,55E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 1/5/1998 8.31E-16 9.00E-14 2.25E-14 4.82E-16 2.00E-14 S.OOE-15 1.77E-16 S.OOE-13 2.25E-13 5.28E-15 6.00E-13 1.50E-13 Not Analyzed Not AI!Piicable Not Applicable 4/28/1998 3.32E-16 9.00E-14 2.25E-14 4.43E-15 2.00E-14 S.OOE-15 :1.11E-16 9.00E-13 2.25E-13 7.43E-15 6.00E-13 1.50E-13 Not Anajyzed Not Applicable Not Applicable 7/31/1998 4.60E-16 9.00E-14 2.15E-14 9,02E-16 Z.OOE-14 S.OOE-15 3.54E-16 9.00E-13 2.25E-13 6.91E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/28/1998 4.08E-16 9.00E-14 2.25E-14 4.93E-16 2.00E-14 S.OOE-15 .2.53E-16 9.00E-13 2.15E-13 4.52E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/28/1998 7.72E-16 9.00E-14 '2.25E-14 3.75E-16 2.00E-14 5.00E-15 3.43E-16 .9.00E-13 2.25E-13 6.73E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/29/1999 5.11E-16 9.00E-14 2.25E-14 4.70E-16 2.00E-14 S.OOE-15 3.70E-16 9.00E-13 2.25E-13 8.96E-15 6.00E-13 1.SOE-13 Not Analyzed Not Applicable Not Applicable 7/3/1999 5.90E-16 9.00E-14 2.25E-14 9.89E-16 2.00E-14 S.OOE-15 L28E-16 9.00E-13 2.25E-13 6,40E-15 6.00E-13 1.50E-13 Not Analyzed Not.Applicable Not Applicable 9/27/1999 1.70E-15 9.00E-14 l .l5E-14 7.SOE-16 2.00E-14 S.OOE-15 4.61E-16 9.00E-13 2.25E-13 7.86E-15 6.00E-13 l.50E-13 Not Analyzed Not Applicable Not Applicable 12/28/1999 1.03E-15 9.00E-14 2.25E-14 7.50E-16 2.00E-14 5.00E-15 z.43E-16 9.00E-13 2.25E-13 6.42E-15 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Ap_plicable 3/27/2000 l.OOE-16 9.00E-14 2.25E-14 2.13E-16 2.00E-14 5.00E-15 2.20E-16 9.00E-13 2.25E-13 5.61E-15 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 6/26/2000 1.75E-16 ~.OOE-14 2.25E-14 3.08E-16 2.00E-14 5.00E-15 l.llE-16 9.00E-13 2.25E-13 3.92E-15 6.00E-13 l.50E-13 Not Analyzed Not Applicable Not Applicable 9/26/2000 3.65E-16 \l.OOE-14 2.25E-14 2.01E-16 2.00E-14 5.00E-15 2.24E-16 9.00E-13 2.25E-13 7.79E-15 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 12/26/2000 2.27E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 4.35E-16 9.00E-13 2.25E-13 8.45E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable !'Jot Applicable 3/26/2001 1.45E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.37E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/2/2001 1.00E-16 9.00E-14 2.l5E-14 1.05E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.99E-15 G.OOE-13 1.SOE-13 Not Analyzed Not Applicable Not Applicable 9/24/2001 1.91E-16 9.00E-14 2.2SE-14 l.OOE-16 2.00E-14 S.OOE-15 2.01E-16 9.00E-13 2.25E-13 8.04E-15 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 12/31/2001 l.38E-16 9.00E-14 2.25E-14 2.05E-16 Z.OOE-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13' 1.83E-15 6.00E-13 1.50E-13 !'Jot Analyzed Not Applicable Not Applicable 4/1/2002 2.20E-16 9.00E-14 2.25E-14 3.38E-16 2.00E-14 5.00E-15 1.26E-16 9.00E-13 2.25E-13 7.48E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/1/2002 1.97E-16 ~.OOE-14 2.25E-14 4,10E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.40E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/30/2002 2.30E-16 9.00E-14 2.25E-14 2.42E-16 2.00E-14 5.00E-15 1.56E-16 9.00E-13 2.25E-13 4.21E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/30/2002 l.OOE-16 9.00E-14 2.25E-14 1.92E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 9.42E-15 G.OOE-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/31/2003 2.50E-16 9.00E-14 1.25E-14 1.69E-16 2.00E-14 S.OOE-15 1.29E-16 9.00E-13 2.25E-13 4.55E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2003 1.00E-16 9.00E-14 2.25E-14 2.87E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 • 2.25E-13 4.20E-15 G.OOE-13 1.50E-13 Not Analyzed Not Applicable Not Applicable - 9/29/2003 1.00E-16 9.00E-14 2.25E-14 8.53E-16 2.00E-14 5.00E-15 3.32E-16 9.00E-13 2.2SE-13 8.69E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/29/2003 ~1.02E-16 9.00E-14 2.25E-14 l.OOE-16 Z,OOE-14 S.OOE-15 1.49E-15 9.00E-13 2.25E-13 9.45E-15 6.00E-13 1.SOE-13 Not Analyzed Not Applicable Not Applicable 3/29/2004 l.OOE-16 9.00E-14 2.25E-14 1,26E-16 2,00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 2,00E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/27/2004 l.OOE-16 9.00E-14 2.25E-14 2.53E-16 2.00E-14 5.00E-15 l.OOE-16 B.OOE-13 2.25E-13 3.23E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/27/2004 l.OOE-16 9.00E-14 2.25E-14 1.15E-16 2.00E-14 S,OOE-15 l.OOE-16 9.00E-13 2.25E-13 9.68E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/27/2004 l.OOE-16 9.00E-14 2.15E-14 2.30E-16 2.00E-14 S.OOE-15 .l.OOE-16 S.OOE-13 2.25E-13 1.37E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/28/2005 l.OOE-16 9.00E-14 l.25E-14 2.66E-16 2.00E-14 S.OOE-15 3.15E-16 9.00E-13 2.25E-13 9.22E-15 G.OOE-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable - 6/29/2005 1.47E-16 9.00E-14 2.25E-14 1.45E-15 2.00E-14 S,OOE-15 1.42E-16 9.00E-13 2.25E-13 9.34E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/26/2005 2.01E-16 9.00E-14 2 25E-14 2.06E-16 2.00E-14 5.00E-15 4.80E-16 9.00E-13 2.25E-13 2.12E-14 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 1/3/2006 4.54E-16 9.00E-14 2.25E-14 1.24E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 3,60E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/3/2006 1.99E-16 9.00E-14 2.25E-14 1.32E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.36E-15 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 7/3/2006 2.76E-16 9.00E-14 2.l5E-14 2,63E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.03E-14 6.00E-13 1.50E-13 Not Analyzed !'Jot Applicable Not Applicable Date Effluent 9E-14 uCi/ml BHV-4U Effluent ZE-14 uCi/ml BHV-4TZ30 Effluent 9E-13 uCi/ml BHV-4R Effluent 6E-13 uCi/ml BHV-4PB Effluent 4e-15 uCi/ml BHV-4T232 Concentration Concentration Concentration Concentration toncentration pmit= limit= limit= limit= Umit= ALARAGoal= 2.25E-14 uCi/ml AlARA Goal-SE-15 uCi/ml ALARAGoal-2.25E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml ALARAGoal-1E-15 uCi/ml Pre 1994 MPC SE-UuCi/ml Pre 1994 MPC BE-14 uCi/ml Pre 1994 MPC 2E-UuCi]ml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable l:lmlt= limit= limit= limit= limit= J>re 1994 1.25E-12 uCi/ml Pre 1994 ALARA SE-13 uCi/ml Pre 1994 1E-12 uCi/ml pre 1994 Not Applicable ALARAGOAl= GOAl= AlARA GOAl= ALARAGOAl= c Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 10/2/2006 4.97E-16 9.00E-14 2.25E-14 2.37E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 1.60E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not ApJllicable 1/1/2007 6.46E-16 9.00E-14 2.25E-14 2.81E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 2.10E-14 6.00E-13 1.50E-13 'Not Analyzed Not Applicable Not Applicable 4/2/2007 7.08E-16 9.00E-14 2.25E-14 3.20E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 1.54E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/2/2007 9.41E-16 9.00E-14 2.25E-14 1.46E-16 2.00E-14 S.OOE-15 1.99E-16 9.00E-13 2.25E-13 2.56E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/30/2007 3.30E·16 9.00E-14 2.25E-14 5.50E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 7.57E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable I 12/31/2007 1.42 E-15 9.00E-14 2.25E-14 1.00E-16 2.00E-14 fi.OOE-15 1.00E-16 9.00E-13 2.25E-13 9.93E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable I 3/31/2008 1.25E-16 9.00E-14 2.25E-14 7.72E·16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 4.09E-15 6.00E-13 1.50E-13 Not Ana[yzed Not Applicable Not Applicable 6/30/2008 1.28E-15 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 3.61E-16 9.00E-13 2.25E-13 1.18E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not JY>_plicable 9/30/2008 2.72E-15 9.00E-14 2.25E·14 l.27E-15 2.00E-14 S.OOE-15 7.66E-16 9.00E-13 2.25E·13 1.10E-14 6.00E-13 1.50E-13 Not Analyzed Not Afl.Piicable Not Applicable 12/31/2008 2.88E-15 9.00E-14 2.25E-14 l.lOE-15 2.00E-14 S.OOE-15 6.56E-16 9.00E-13 2.25E-13 1.38E·14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/15/2009 1.56E-15 9.00E-14 2.25E-14 4.57E-16 2.00E-14 S.OOE-15 2.99E-16 9.00E-13 2.25E-13 4.97E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/15/2009 5.67E-17 9.00E-14 2.25E-14 2.17E-16 2.00E-14 S.OOE-15 1.51E-16 9.00E-13 ·2.25E-13 4.47E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/15/2009 4.05E-15 9.00E-14 2.25E-14. 1.45E·15 2.00E-14 S.OOE-15 2.52E-16 9.00E-13 2.25E-13 1.24E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/15/2009 6.50E·15 9.00E-14 2.25E-14 3.48E-16 2.00E-14 S.OOE-15 1.33E-16 9.00E-13 2.25E-13 7.60E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/31/2010 6.01E·15 9.00E-14 2.25E-14 1.26E-16 Z.OOE-14 S.OOE-15 1.3!1E-16 9.00E-13 2.25E-13 1.19E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2010 2.33E-15 9.00E-14 2.25E-14 7.29E·16 2.00E-14 S.OOE-15 2.66E-16 9.00E-13 2.25E-13 3.27E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Afl.Piicable 9/30/2010 4.77E-15 9.00E-14 2.25E-14 1.80E-15 2.00E-14 fi.OOE-15 8.23E-16 . 9.00E-13 ~.25E-13 5.11E·15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/31/2010 3.93E-15 9.00E-14 2.25E-14 3.90E·16 2.00E-14 S.OOE-15 2.56E-16 9.00E-13 2.25E-13 1.13E·14 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 4/4/2011 1.29E·15 9.00E-14 2.25E-14 1.40E-16 2.00E-14 S.OOE-15 1.58E·16 9.00E-13 2.25E-13 1.11E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not l!.pplicable 7/4/2011 3.30E-15 9.00E-14 2.25E·14 5.44E-16 2.00E-14 5.00E-15 4.18E-16 9.00E-13 2.25E-13 8.26E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 10/3/2011 1.32E-15 9.00E-14 2.25E-14 7.89E-16 2.00E-14 S.OOE-15 1.28E-16 9.00E-13 2.25E·l3 l.lSE-14 6.00E-13 1.50E-l3 Not Analyzed Not Applicable Not Applicable 1/3/2012 1.04E-15 9.00E-14 2.25E-14 3.25E-16 2.00E-14 5.00E-15 !2.28E-16 9.00E-13 2.25E-13 1.14E-14 6.00E-13 1.50E-13 Not Analyzed Not Ap_plicable Not Applicable 4/3/2012 2.51E-15 9.00E-14 2.25E-14 5.02E-16 2.00E-14 5.00E-15 2.27E-16 9.00E-13 2.25E-13 1.03E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/2/2012 2.62E-15 9.00E-14 2.25E-14 1.23E·15 2.00E-14 S.OOE-15 2.97E-16 9.00E-13 2.25E-13 9.27E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 10/1/2012 4.05E-15 9.00E-14 ;z.25E-14 8.33E-16 2.00E-14 5.00E-15 :>.43E-16 9.00E-13 2.25E-13 1.21E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/31/2012 2.32E·15 I,!.OOE-14 2.25E-14 5.89E-16 2.00E-14 5.00E-15 3.75E-16 9.00E-13 2.25E-13 1.56E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/25/2013 B.04E-15 '9.00E-14 2.25E-14 4.99E-16 2.00E-14 S.OOE-15 2.79E-16 9.00E-13 2.25E-13 2.13E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/2/2013 2.50E-15 ~.OOE-14 2.25E-14 3.62E-16 2.00E-14 S.OOE-15 2.40E-16 9.00E-13 2.25E-13 4.93E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not l!.pplicable 9/30/2013 2.98E·15 9.00E-14 7.25E-14 4.49E-16 2.00E-14 S.OOE-15 '1.54E-16 9.00E-13 2.25E-13 7.49E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/30/2013 ;3.88E-15 9.00E-14 2.25E-14 1.03E·16 2.00E-14 5.00E-15 4.47E-17 9.00E-13 2.25E-13 2.93E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/31/2014 4.69E-15 9.00E-14 2.25E-14 1.37E-16 2.00E-14 5.00E-15 3.53E-16 9.00E-13 .2.25E-13 l.OSE-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2014 4.16E-15 9.00E-14 2.25E-14 6.96E-16 2.00E-14 5.00E-15 1.77E-15 9.00E-13 2.25E-13 1.06E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not AP,plicable 9/30/2014 6.56E-15 9.00E-14 2.25E-14 2.73E-16 2.00E-14 S.OOE-15 2.77E-16 9.00E-13 2.25E-13 1.11E-14 6.00E-13 1.50E-13 1.01E-17 4.00E-15 1.00E-15 12/29/2014 2.00E·16 9.00E-14 2.25E-14 4.00E-17 2.00E-14 S.OOE-15 4.00E-17 9.00E-13 2.25E-13 1.90E-14 6.00E-13 1.50E-13 l.OOE-17 4.00E-15 1.00E-15 3/30/2015 ,5.90E-15 9.00E-14 2.25E-14 ?.OOE-17 2.00E-14 S.OOE-15 1.00E-16 · 9.00E-13 2.25E-13 2.80E-14 6.00E-13 1.50E-13 5.00E-19 4.00E-15 1.00E-15 6/29/2015 l.SOE-15 9.00E-14 2.25E·14 l.OOE-16 2.00E-14 S.OOE-15 2.00E-16 9.00E-13 2.25E·13 1.20E-14 6,00E-13 1.50E·13 1.00E-17 4.00E-15 1.00E-15 9/28/2015 5.00E-15 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 7.00E·15 6.00E-13 1.50E-13 7.00E·18 4.00E-15 l.OOE-15 12/28/2015 4.SOE-16 9.00E-14 2.25E-14 7.00E-17 2.00E-14 S.OOE-15 6.00E-17 9.00E-13 2.25E-13 2.00E-14 6.00E-13 1.50E-13 S.OOE-19 4.00E-15 l.OOE-15 3/28/2016 p.OOE-16 9.00E-14 2.25E-14 2.00E-17 2.00E-14 S.OOE-15 5.00E-17 9.00E-13 2.25E-13 1.70E-14 6.00E-13 1.50E-13 2.00E-18 4.00E-15 1.00E-15 6/27/2016 ;!.90E-15 9,00E-14 2.25E-14 5.00E-17 2.00E-14 S.OOE-15 4.00E-16 9.00E-13 2.25E-13 8.80E-15 6.00E-13 1.50E-13 S.OOE-18 4.00E-15 1.00E-15 9/27/2016 6.20E-15 9.00E-14 2.25E-14 4.40E-16 2.00E-14 S.OOE-15 2.20E-15 9.00E-13 e.25E-13 3.40E·16 6.00E-13 1.SOE-13 7.10E·18 4.00E-15 l.OOE-15 12/27/2016 4.10E·15 9.00E-14 2.25E-14 3.00E·16 2.00E-14 S.OOE-15 4.80E·16 9.00E-13 2.25E-13 2.20E-14 6.00E-13 1.50E-13 4.50E-18 4.00E-15 1.00E-15 -- (Log Scale) ...... ...... ...... ...... 0 0 0 0 0 0 0 0 m m m m I I I I ...... ...... ...... ...... 00 --.1 CJ) c.n Sep-81 ' .. ~ Sep-82 • Sep-83 Sep-84 Sep-85 00::: Sep-86 4 _:~f-. + Sep-87 Sep-88 ....._ .... ., -c Sep-89 .... lll ::::l ~ ti~ c Sep-90 3 ~ z Sep-91 lll -Sep-92 c .... ~ I• .. Sep-93 + Sep-94 -i Sep-95 -* li - ~ 0 Sep-96 :::::!. • []I c 3 Sep-97 r\J w Sep-98 0 + Sep-99 Sep-00 ~ I• .. • - ~ -r'l '\1 .. p ~ ~ ~ ~ ~~ JJ Sep-01 lll 9: c Sep-02 3 r\J Sep-03 I\) ~ f'~ .oo::::; ~ ~ CJ) Sep-04 . ...--:.. ~ .. -.::: + Sep-05 r Sep-06 CD lll Sep-07 a. r\J ~ ~ r- ~ ...... Sep-08 0 + Sep-09 Sep-10 -i Sep-11 ~ 0 :::::!. Sep-12 c 3 r\J Sep-13 w I\) Sep-14 iii" .... ~ ~ ....-~ Ml:: -~ '--~:- .-::::::: ~ ~ p ~ ~ ~ ~ ~ ~~ ~ r; ... ~ _,_. ~ ~~ Sep-15 ~ • oc:: =:::::; ,._ Sep-16 -.. L -- ...... 0 0 m I ...... ""'" ~ ~ -'~ ... ~ I-" :-:::::,~ r.. ,.,.., I"" .~ ..... ;_...J ~ ~ F-~ .:2 ~ ~ p ~ ~ t> ~ > ~ ~ ~ ~ ~ ~ .... ~ ~~ i="' h t>l ~ :::::¥ ...... 0 0 m I ...... w ~~~~~~ t::-~ ~ ~ ...... 0 0 m I ...... I\) tD ::I: -;:: ~ :D I» Q. 0 ::::s s::::: (") Q. CD 0 0 ::::s (") CD ::::s -""' I» !:!: 0 ::::s Ul -s::::: 0 :::::.: 3 ..:::: 1.00E-11 1.00E-12 1.00E-13 Q) (U (.) Ul.OOE-14 Cl 0 ::::!- 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit= 9E-14 uCi/ml ALARA Goal= 2.25E-14 uCi/ml Pre 1994 MPC Limit= 5E-12uCi/ml Pre 1994 ALARA Goal = 1.25E-12 uCi/ml t ~~ ~ ..... v • ~ f ~ ~ 1 \ .... ..... r ' i ,., ..,£ ~ ' BHV-4 Uranium-Natural Concentrations (uCi/ml) . "71ooc ..... ..-. . ~ i/ "l • !I .... 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N ~s:: • i-<1'- :~ ... .... ~ ~ .... • ~ l.() .-uJ 0 ~ ..- ~ ~ ._. ~ ~ , '"--1 ~ ~ :::: ~ ~ t; tO .-I w 0 ~ ::>oi ,_, - - - I'-.-I w 0 ~ g~-das 9~-das 17 ~-das 8~-das G~-das ~ ~-das o~-das 6o-das so-das Lo-das go-d as go-d as 17o-das 8o-das GO-das ~o-des oo-das 66-das 95-das L6-das 95-das 96-das 175-das 86-das G6-das ~6-das 06-das 6s-das ss-das La-das gg-das gg-das 179-das 88-das Gs-das ~a-d as ::=- .E 0 :J -In c 0 '; f! -c Q) u c 0 0 co N N I E :J "C C'CI a: ~ ::> J: al ,.... ...... I w 0 C! ,.... ,_.,. I-"" C\J ,.... I w 0 C! L.o.. ~~ t-" r--- I• F+- 41 ~ 11 1--~ ~'--+-p.4 ~ (") """ I!) ,.... ...... ,.... I I I w w w 0 0 0 C! 0 0 ,.... ~areos Bo1f < ~" ....- ~~ ::::. .. ,. .. ~ ~~ .. --. < =:-....... ~0::::: ~ ...... ~ ~ c:~ >t <!~ !~ ~ 4 ~ "':-..... • ;;: •::::;jj - --... ...... .... ,.... ... ,..;;;;>"~! CD ,.... I w 0 0 ~ • I'-,.... I w 0 C! - - - - <X) ,.... I w 0 C! ,.... 9~-das 9~-das v~-das 8~-das G~-das ~ ~-das o~-das 6o-das so-das La-das 9o-das 9o-das ro-d as 8o-das Go-d as ~a-d as oo-das 66-das 86-das L6-das 95-das 96-das 175-das 86-das G6-das ~6-das 06-das 6s-das ss-das Ls-das 99-das 99-das vs-das 88-das GS-das ~s-das -E ::::: 0 :::s -w t: 0 ... ca ... -t: Q) (,) t: 0 0 0 T"" N I "C ca Q) ..J ~ ::> :I: m uJ 0 C? ..... C\J (") ..... I uJ w 0 0 C? C? ..... ~ b k:; ~ ·~ ~ ::.-: , ~ ~ ~ ...... r-- ~ ~t::.o ~ • • t::t 4 < ~ 4 ~ I• 0:::::: ~ • §: 1~1"= ~ 1- ~ i"""" ~ ~-~ I' ~ p. , 4F-. ........ ~ ..... p. ) "<t ,-- I w 0 0 (a1e~s oo1) • L{) <0 ..... ..... I I w w 0 0 C? C? ..... - - - - - t--..... I w 0 C? 9~-das s~-das v~-das 8~-das l~-das ~ ~-das o~-das 6o-das so-das Lo-das so-das so-das vo-das 8o-das lO-das ~o-das oo-das 66-das 86-das L6-das 96-das S6-das v6-das 86-das l6-das ~6-das 06-das 68-das ss-das Ls-das ss-das ss-das vs-das 8s-das ls-das ~s-das Sep-14 Oct-14 Nov-14 Dec-14 Jan-15 Feb-15 Mar-15 Apr-15 May-15 Jun-15 Jul-15 Aug-15 Sep-15 Oct-15 Nov-15 Dec-15 Jan-16 Feb-16 Mar-16 Apr-16 May-16 Jun-16 Jul-16 Aug-16 Sep-16 Oct-16 Nov-16 Dec-16 0 0 m I _. co - - - - - - _.. _.. 0 0 0 0 m m I I _. _. CX> --.1 v v"' v ~ ~ I', ~ I / v / 1\ \ 1\ \ • (Log Scale) _.. _.. 0 0 0 0 0 0 m m m I I I _. _.. _.. 0) (]1 ~ _.. 0 0 r:n _.. w )>m r-::::1: l>c :D ID l>::!, G>o 0 0 Ill :I jj"~ .... :I o :: m el. I -• .... 0 Cll ::::s f,C -· 3 [; ""' m .!.. (11 c::: 0 :::.: ~ aJ ::I: ~ ~ -t ::r 0 :::::!. c 3 I 1\) w 1\) 0 0 ::::s (') CD ::::s -""' a ()' ::::s tn -c 0 ~ ..:::: TABS BHV-5 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent 9E-14 uCi{ml BHV-5U Effluent 2E-14 uCi/ml liHV-ST230 Effluent 9E-13 uCi/ml BHV-5R Effluent 6E-13 uCi/ml BHV-5PB Effluent 4e-15 uCi/ml BHV-51232 Concentration Concentration Concentration Concentration Concentration I limit= limit= limit= limit= limit= I ALARAGoal= 2.25E-14 UCi/ml ALARA Goal= SE-15 uCi/ml /'LARA Goal -2.25E-13 uCi/ml ALARA Goal-1.5E-13 uCi/ml AlARAGoal = 1E-15 uCi/mi Pre1994MPC 5E-UuCi/ml Pre 1994 MPC SE-14 uCi/ml Pre 1994 MPC 2E-12 uCi/ml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable limit= limit= Limit= limit= limit= I Pre 1994 1.25E-1z uei/ml Pre 1994 5E-13 uCi/ml Pre 1994 AlARA I 1E-12 uCi/ml Pre 1994 Not Applicable ALARAGOAL= ,t>.LARA GOAL = GOAL= ALARAGOAL= Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 _2.44E-15 S.OOE-12 1.25E-12 1.53E-15 8.00E-14 2.00E-14 7.54E-16 2.00E-12 5.00E-13 1.69E-14 4.00E-12 1.00E-12 Not Analyzed Not Ap_11licable . ]'Jot AI'Jllicable 12/14/1981 4.84E-15 S.OOE-12 1.25E-12 2.78E-15 8.00E-14 Z.OOE-14 1.84E-15 2.00E-12 5.00E-13 1.53£-14 4.00£-12 1.00£-12 Not Analyzed Not Applicable Not Applicable 3/29/1982 1.04E-15 S.OOE-12 1.25E-12 2.62E-15 8.00£-14 2.00E-14 1.11E-15 2.00E-12 5.00E-13 2.98E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 6/30/1982 3.61E-15 S.OOE-12 1.25E-12 7.61E·15 8.00E-14 2.00E-14 1.39E-15 2.00E-12 5.00E-13 1.80E-15 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 9/27/1982 1.71E-14 S.OOE-12 1.25E-12 9.46E-15 8.00E-14 2.00E-14 3.80E·15 2.00E-12 5.00E-13 2.35£-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 1/3/1983 1.90£-14 S.OOE-12 1.25E-12 5.77£-15 8.00£-14 2.00£-14 9.34E-17 2.00E-12 5.00E-13 4.32E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 4/4/1983 S.OOE-12 1.25E-12 2.33E-15 8.00E-14 2.00E-14 5.93E-16 2.00E-12 5.00E-13 3.01E-14 4.00E-12 l.OOE-12 Not Analyzed Not Ap~licable Not Applicable 6/30/1983 7.62E-16 5.00E-12 1.25E-12 3.25E-15 8.00E-14 2.00E-14 6.28E-15 2.00E-12 5.00£-13 2.69£-14 4.00E-12 1.00E-12 Not Analyzed · Not Applicable Not Applicable 10/3/1983 4.86E-16 S.OOE-12 1.25E-12 1.10£-15 S.OOE-14 2.00£-14 3.63E-16 2.00£-12 5.00E-13 2.08£-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 1/3/1984 6.96E-15 5.00E-12 1.25E-12 9.69E-16 8.00E-14 2.00£-14 9.60£-16 ·-2.00E-12 5.00E-13 1.83E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 4/2/1984 1.64E-15 S.OOE-12 1.25E-12 1.34E-15 8.00E-14 2.00E-14 3.88E-15 2.00E-12 5.00E-13 4.67£-14 4.00E-12 l.OOE-12 Not Analyzed Not Ap~licable Not AI'Jllicable 7/2/1984 1.12E-15 S.OOE-12 1.25E-12 1.92E-15 8.00E-14 2.00E-14 3.31E-15 "2.00E-12 S.OOE-13 2.21E-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Ap_plicable 10/1/1984 1.11E-15 5.00E-12 1.25E-12 3.13E-16 8.00E-14 Z.OOE-14 4.21E-16 ; 2.00E-12 5.00E-13 1.57E-14 4.00E-12 l.OOE-12 Not Analyzed f>jot Applicable Not Applicable 1/2/1985 7.32E-16 5.00E-12 1.25E-12 6.71£-16 8.00E-14 2.00E-14 4.94£-16 2.00E-12 5.00E-13 2.42£-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Jllot Applicable 4/1/1985 2.36E-16 5.00E-12 1.25E-12 5.43E-16 8.00E-14 2.00E-14 2.71E-16 2.00£-12 5.00£-13 1.25£-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 7/1/1985 7.58E-16 S.OOE-12 1.25E-12 4.00£-16 8.00£-14 2.00£-14 6.90£-16 2.00E-12 5.00£-13 2.15£-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Ap_plicable 9/30/1985 7.47E-15 S.OOE-12 1.25£-12 1.16£-15 8.00£-14 2.00£-14 2.19£-15 , 2.00E-12 5.00E-13 9.20£-15 4.00£-12 1.00£-12 Not Analyzed Not Applicable Not Applicable 1/2/1986 1.75E-14 5.00E-12 1.25E-12 7.24£-15 S.OOE-14 2.00£-14 3.83£-15 2.00E-12 5.00£-13 1.13£-16 4.00£-12 1.00£-12 NOt Analyzed Not Applicable Not Applicable 4/1/1986 2.99E-14 5.00£-12 1.25E-12 7.64£-15 8.00£-14 2.00£-14 1.51£-14 . 2.00£-12 5.00£-13 2.22£-14 4.00£-12 1.00£-12 Not Analyzed Not Applicable Not Applicable 6/30/1986 2.23E-14 5.00£-12 1.25E-12 5.19£-15 8.00£-14 2.00[-14 1.05E-14 2.00£-12 5.00E-13 2.16£-14 II.OOE-12 l.OOE-12 Not Ana]yzed Not Applicable Not Applicable 10/27/1986 2.33E-14 · S.OOE-12 1.25E-12 7.78£-15 S.OOE-14 2.00£-14 1.60£-14 . 2.00£-12 5.00£-13 2.02£-14 4.00E-12 l.OOE-12 Not Analyzed Not AI'Jllicable ·Not Ap_plicable 12/15/1986 3.40E-14 5.00E-12 1.25E-12 5.35£-15 8.00E-14 2.00£-14 l.47E-14 2.00E-12 S.OOE-13 2.82£-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 3/16/1987 2.06E-14 S.OOE-12 1.25E-12 4.50E-15 8.00£-14 2.00E-14 6.74E-15 2.00E-12 5.00E-13 7.29£-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/11/1987 2.SOE-14 5.00E-12 1.25£-12 8.54E-15 8.00£-14 2,00E-14 8.15E-15 2.00E-12 5.00E-13 3.28£-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 9/9/1987 2.65E-14 5.00E-12 1.25E-12 6.62E-15 8.00£-14 2.00E-14 9.34E-15 2.00E-12 5.00E-13 2.77E-14 4.00£-12 1,00£-12 Not Analyzed Not Applicable Not Applicable 11/2/1987 1.80E-14 5.00E-12 J..25E-12 7.09E-15 8.00£-14 2.00E-14 ;7.20E-15 . 2.00E-12 5.00E-13 1.77E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/16/1988 1.01E-14 S.OOE-12 1.25E-12 2.98E-15 8.00£-14 2.00E-14 3.93E-15 2.00E-12 5.00E-13 3.36E-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/18/1988 1.78E-14 5.00E-12 1.25E-12 8.14E-15 8.00£-14 2.00£-14 7.43E-15 2.00E-12 5.00E-13 2.12E-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/15/1988 1.79E-14 5.00E-12 1.25E-12 1.49£-14 8.00£-14 2.00£-14 5.34E-15 2.00E-12 5.00E-13 2.45E-14 II.OOE-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/14/1988 4.46E-14 5.00E-12 1.25E-12 1.39E-14 8,00£-14 2.00E-14 ,l.17E-14 2.00E-12 5.00E-13 3.43E-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/13/1989 1.67E-14 S.OOE-12 1.25E-12 5.54E-15 8.00£-14 2.00E-14 7.20E-15 2.00E-12 5.00E-13 5.02E-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/15/1989 2.03E-14 5.00E-12 1.25E-12 7.05E-15 8.00E-14 2.00E-14 9.56£-16 2.00E-12 5.00E-13 1.43E-14 4.00£-12 l.OOE-12 Not Analyzed Not A_pplicable Not Applicable 8/14/1989 2.81£-15 5.00£-12 1.25£-12 3.78E-15 8.00E-14 2.00E-14 9.26£-15 2.00E-12 5.00E-13 1.50E-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/13/1989 5.38E-14 5.00E-12 1.25E-12 8.01E-15 8.00E-14 2.00E-14 1.81E-14 2.00E-12 5.00E-13 4.09E-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Ap_plicable 2/12/1990 4.48E-14 :;.ooE-12 1.25E-12 1.48E-14 8.00E-14 2.00£-14 1.28E-14 2.00E-12 S.OOE-13 3.88E-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/14/1990 2.18E-14 5.00E-12 1.25E-12 1.70E-14 8.00E-14 2.00E-14 1.59E-14 2.00E-12 5.00E-13 3.49E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/13/1990 9.53E-15 S.OOE-12 1.25E-12 1,70E-14 8.00£-14 2.00E-14 3.27E-15 2.00E-12 5.00E-13 1.27E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/12/1990 1.11E-14 5.00E-12 1.25E-12 5.27E-15 8.00£-14 l.OOE-14 5.38E-15 2.00E-12 5.00E-13 1.56E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/11/1991 6.3SE-16 S.OOE-12 1.25E-12 3.13E-16 8.00E-14 2.00E-14 2.31E-16 2.00E-12 5.00E-13 3.89£-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/13/1991 1.22£-15 S.OOE-12 1.25E-12 6.14E-15 8.00£-14 2.00E-14 4.41E-15 2.00E-12 ·s.OOE-13 2.50£-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/12/1991 7.84E-16 5.00E-12 1.25E-12 1.43E-15 8.00£-14 2.00E-14 4.47E-16 2.00E-12 5.00E-13 1.84E-14 4,00£-12 l .OOE-12 Not Analyzed Not Applicable Not Applicable 11/11/1991 5.37E-16 5.00E-12 1.25E-12 4.20E-16 8.00E-14 2.00E-14 1.37E-16 2.00E-12 S.OOE-13 1.27E-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/10/1992 3.54E-16 5.00E-12 1.25E-12 l.lSE-16 8.00E-14 2.00E-14 4.08E-17 2.00E-12 S.OOE-13 3,69E-14 4.00£-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 5/11/1992 4.71E-16 5.00E-12 1.25E-12 9.58E-16 8.00£-14 2.00E-14 8.31E-17 2.00E-12 5.00E-13 1.43E-14 4.00£-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 8/10/1992 5.32E·15 5.00E-12 1.25E-12 3.36E-16 8.00£-14 2.00E-14 1.65E-16 2.00E-12 5.00E-13 1.59E-14 4.00£-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 11/9/1992 3.66E-16 5.00£-12 1.25E-12 2.25E-16 8,00£-14 2.00E-14 l .OSE-16 2.00E-12 p.OOE-13 2.24E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 2/9/1993 2.0SE-16 5.00E-12 1.25E-12 9.14E-17 8.00E-14 2.00E-14 6.31E-17 2.00E-12 S.OOE-13 3.41E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/10/1993 4.80E-16 5.00E-12 1.25E-12 8.25£-16 S,OOE-14 2.00E-14 1.26E-15 2.00E-12 5.00E-13 1.83E-14 4,00E-12 l.OOE-12 Not Analyzed Not Applicable )\Jot Applicable 8/10/1993 8,30E-16 5.00E-12 1.25E-12 1.90E-16 S.OOE-14 2.00£-14 2.10E-16 2.00E-12 S.OOE-13 1.70E-14 4.00£-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable Date Effluent 9E-14 uCi/ml BHV·SU Effluent ZE-14 uCi/ml BHV-ST230 Effluent 9E-13 uCi/ml BHV-SR Effluent 6E-13 uCi/ml I!HV-SPB Effluent 4e-15 uCi/ml -BHV-ST232 Concentration Concentration Concentration Concentration Concentration Limit= Limit = Limit= Limit= Limit= ALARAGoal= 2.2SE-14 uCi/ml ALARA Goal= SE-15 uCi/ml ALARAGoal= i!-25E-13 uCi/ml ALARA Goal= 1.SE-13 uCi/ml ALARA Goal = ' lE-15 uCi/ml Pre 1994 MPC SE-12 uCi/ml Pre 1994 MPC SE-14 uCi/ml pre 1994MPC 2E-12 uCi(ml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable Limit= limit= Limit= Limit= Limit= Pre 1994 1.25E-12 uCi/ml pre 1994 SE-13 uCi/ml Pre 1994 ALARA 1E-12 uCi/ml Pre 1994 Not Applicable ALARAGOAL= ALARAGOAL= GOAL= ALARAGOAL= Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone ~FC EFCA 11/8/1993 2.7DE-16 5.00E-12 1.25E-12 8.00E-17 8.00E-14 2.00E-14 7.00E-17 Z.OOE-12 5.00E-13 2.34E-14 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Ap_plicable 2/7/1994 3.18E-16 5.00E-12 1.25E-12 l.OOE-16 8,00E-14 2.00E-14 5.18E-16 2.00E-12 5.00E-13 3.64E-14 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 5/9/1994 1.80E·l5 S.OOE-12 1.25E-12 9.78E-16 8.00E-14 2.00E-14 l.lOE-15 2.00E-12 5.00E-13 8.30E-15 4.00E-12 1.00E-12 !'Jot Analyzed Not Applicable Not Applicable 8/9/1994 2.67E·l5 5.00E-12 l.ZSE-12 1.11E-15 8.00E-14 2.00E-14 4.95E·l6 2.00E-12 5.00E-13 l.OOE-16 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/7/1994 9.21E-17 5.00E-12 1.25E-12 1.59E-15 8.00E-14 2.00E-14 1.66E-15 Z.OOE-12 S.OOE-13 l.OOE-16 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/7/1995 1.51E·15 9.00E-14 2.25E-14 9.50E-16 2.00E-14 5.00E-15 9.70E-17 9.00E-13 2.25E-13 9.35E·15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not AmJiicable 5/9/1995 l .21E·16 9.00E-14 2.2SE-14 8.56E-16 Z.OOE-14 5.00E-15 3,06E-15 9.00E-13 2.25E-13 4.34E-15 G.OOE-13 1,50E-13 Not Anajyzed Not A!!!>licable Not Applicable 8/9/1995 1.66E-16 9.00E-14 2.25E-14 1.67E·15 z.OOE-14 S.OOE-15 3.90E-15 9.00E-13 2.25E-13 5.60E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 11/11/1995 2.04E·14 9.00E-14 2.25E-14 6.70E-15 l.OOE-14 5.00E-15 7.65E-15 9.00E-13 2.25E-13 4.47E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable l /5/1996 4.50E-14 9.00E-14 2.25E-14 3.58E-14 2.00E-14 S.OOE-15 2.39E·l4 9.00E-13 2.25E-13 7.30E-15 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable I 5/6/1996 1.76E-15 9.00E-14 :2.25E-14 3.57E·15 2.00E-14 5.00E-15 9.55E·16 9.00E-13 2.25E-13 7.54E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 8/5/1996 2.37E-15 9.00E-14 2.25E-14 8,18E·15 2.00E-14 5.00E-15 7.46E-16 9.00E-13 2.25E-13 5.75E-15 G.OOE-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 11/6/1996 3.53E-15 9.00E-14 ~.25E-14 5.31E·15 2.00E-14 5.00E-15 9.39E-16 9.00E-13 2.25E-13 1.21E·14 6.00E-13 1.50E-13 Not Analyzed Not A(l,~icable Not Applicable 2/6/1997 1.84E-16 9.00E-14 ~.25E-14 2.01E-16 2.00E-14 5.00E-15 1.87E-16 9.00E-13 2.25E-13 6.14E-15 6,00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 5/5/1997 5.75E-16 9.00E-14 2.25E-14 7.24E-16 2.00E-14 5.00E-15 6.07E-16 9.00E-13 2.25E-13 4,75E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 8/11/1997 1.21E-15 9.00E-J.4 2.25E-14 7.39E-16 2.00E-14 S.OOE-15 5.05E-16 9.00E-13 2.25E-13 4.92E-15 6.00E-13 1.50E-13 Not Analyzed Not ApQiicable Not ApJ1Iicable 1/5/1998 9.89E-16 9.00E-14 2.25E-14 1.92E·15 2.00E-14 S.OOE-15 6.21E·16 9.00E-13 2.25E-13 4.68E·15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/28/1998 2.84E-15 '9.00E-14 2.25E-14 2.38E-15 2.00E-14 S.OOE-15 1.72E-15 9.00E-13 2.25E-13 7,35E·15 G.OOE-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/31/1998 7.49E-16 .9.00E-14 2.25E-14 1.49E-15 Z.OOE-14 S.OOE-15 8.34E-16 9.00E-13 2.25E-13 7.01E-15 G.OOE-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/28/1998 1.07E·15 9.00E-14 2.25E-14 9.20E-16 2.00E-14 5.00E-15 6.32E·16 IJ.OOE-13 2.25E-13 3.95E-15 G.OOE-13 1.50E-13 Not Analyzed NOt Applicable Not Applicable 12/28/1998 8.51E·15 9.00E-14 2.25E-14 4.58E-15 2.00E-14 5.00E-15 4.58E-15 9.00E-13 2.25E-13 1.43E-14 6.00E-13 1.50E-13 Not Analyzed jllot Applicable Not Applicable 3/29/1999 3.75E-15 9.00E-14 2.25E-14 2.45E·15 2.00E-14 S.OOE-15 2.39E-15 9.00E-13 2.25E-13 8.46E·15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/3/1999 1.53E-15 9.00E-14 2.25E-14' 8.65E-16 2.00E-14 S.OOE-15 6.52E·16 9.00E-13 2.25E-13 7.20E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/27/1999 ':S.83E-15 9.00E-14 2,25E-14 3.52E·15 2.00E-14 5.00E-15 2.55E-15 9.00E-13 2,25E-13 8.22E·15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/28/1999 9.48E-15 9.00E-14 2.25E-14 6.20E-15 2.00E-14 5.00E-15 3.96E-15 9.00E-13 2.25E-13 7.56E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/27/2000 2.06E·15 9.00E-14 2.25E-14 1.27E-15 2.00E-14 S.OOE-15 1.09E·15 9.00E-13 2.25E-13 7.72E-15 6.00E-13 1.50E-13 jllot Analyzed Not Applicable Not Applicable 6/26/2000 1.50E-15 9.00E-14 2.25E-14 1.24E-15 Z.OOE-14 5.00E-15 1.01E·15 9.00E-13 2.25E-13 4.36E-15 G.OOE-13 1.SOE-13 Not Anal-,.zed Not Ap_plicable Not Applicable 9/26/2000 1.04E-15 9.00E-14 2.25E-14, .5.45E-16 2.00E-14 5.00E·15 6.01E·16 9.00E·13 . 2.25E-13 7.67E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/26/2000 1.48E·15 9.00E-14 2.25E-14 7.56E-16 2.00E-14 5.00E-15 6.84E·16 9.00E·13 2.25E-13 7.00E·15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/26/2001 4.27E·16 9.00E-14 2.25E-14 2.19E-16 2.00E-14 5.00E-15 1.89E-16 9.00E-13 2.25E-13 6.13E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not AI>plicable 7/2/2001 4.52E·16 9.00E-14 2.25E-14 4.02E-16 2.00E-14 5.00E-15 l.OOE·16 9.00E-13 2.25E·13 7.48E·15 6.00E-13 1.50E·13 Not Analyzed Not Applicable Not Applicable 9/24/2001 ~.65E·16 9.00E-14 2.25E-14 2.06E-16 Z.OOE-14 S.OOE-15 2.02E·16 9.00E-13 2.25E-13 6.98E·15 G.OOE-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/31/2001 7.40E-16 9.00E-14 2.25E-14 3.51E-16 Z.OOE-14 5.00E-15 3.64E·16 9.00E-13 ~.25E-13 4.72E-15 G.OOE-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/1/2002 1.26E·15 9.00E-14 2.25E-14 7.53E-16 2.00E-14 5.00E-15 7.19E-16 9.00E-13 2.25E-13 9.65E-15 G.OOE-13 1.50E-13 Not Analyzed Not Applicable Not Al)plicable 7/1/2002 1.02E-15 9.00E-14 2.25E-14 1.03E-15 2.00E-14 S.OOE-15 3.39E·l6 9.00E-13 2.25E·l3 7.20E·15 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 9/30/2002 5.82E·16 9.00E-14 2.25E-14 9.28E-16 2.00E-14 5,00E-15 3.14E-16 9.00E-13 2.25E-13 4.48E·15 6.00E-13 1.50E-13 .Not Analyzed Not Applicable Not Applicable 12/30/2002 l.OOE-16 9.00E-14 2.25E-14 7.67E·16 2.00E-14 5,00E-15 3.48E-16 9.00E-13 2.25E-13 9.56E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/31/2003 1.13E-15 9.00E-14 2.25E-14 7.41E·16 Z.OOE-14 5,00E-15 4.41E-16 9.00E-13 l.25E-13 6.68E-15 G.OOE-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2003 4.35E-16 9.00E-14 .. 2.25E-14 5.08E·16 2.00E-14 5.00E-15 2.51E·16 9.00E-13 12.25E-13 l.34E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/29/2003 1.51E·16 9.00E-14 2.25E-14 1.02E·16 2.00E-14 5.00E-15 l.OOE-16 !J.OOE-13 '2.25E-13 7.28E·15 6.00E-13 1.50E-13 Not Analyzed Not Applicable , Not Applicable 12/29/2003 1.52E·16 9.00E-14 2.25E-14 1.54E-16 2.00E-14 5.00E-15 1.51E·16 9.00E-13 2.25E-13 7.02E·15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/29/2004 l.OOE-16 9.00E-14 2.25E-14 1.12E-16 2.00E-14 S.OOE-15 1.00E·16 9.00E-13 2.25E-13 8.82E-15 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 6/27/2004 l.lSE-16 9.00E-14 2.25E-14 3.11E-16 2,00E-14 5.00E-15 1.25E-16 9.00E-13 .2.25E-13 2.47E-15 6.00E-13 1.50E-13 Not Analyzed Not Apj>licable Not Applicable 9/27/2004 1.16E-16 ~.OOE-14 2.25E-14 1.72E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25Ec13 l.lOE-14 6.00E-13 l.SOE-13 Not Analyzed Not Applicable . Not Applicable 12/27/2004 1.14E·16 9.00E-14 2.25E-14 1.06E·16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 1.59E·14 6,00E-13 1.SOE-13 Not Analyzed Not Applicable Not Applicable 3/28/2005 1.00E-16 9.00E-14 2.25E-14 2.04E-16 Z.OOE-14 5.00E-15 1.83E-16 9.00E-13 2.25E-13 8.57E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/29/2005 1.83E-16 9.00E-14 2.25E-14 3.81E-16 2.00E-14 5.00E-15 3.09E-16 :J.OOE-13 2.25E-13 1.06E·14 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 9/26/2005 2.87E-16 9.00E-14 2.25E-14 8.21E-16 Z.OOE-14 5,00E-15 3.71E-14 9.00E-13 2.25E-13 6.28E-14 G.OOE-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 1/3/2006 8.74E·16 9.00E-14 2.25E-14 3.79E-16 2.00E-14 5.00E-15 1.31E-16 9.00E-13 2.25E-13 4.32E·14 6.00E-13 1.50E-13 Not~alyzed Not Api>Iicable Not A!!!>licable Date Effluent ~E-14 uCi/ml BHV-SU Effluent ZE-14 uCi/ml BHV-5T230 Effluent 9E-l3 uCi/ml BHV-SR Effluent 6E-l3 uCi/ml BHV-SPB Effluent 4e-15 uCi/ml BHV-5T232 Concentration Concentration Concentration Concentration Concentration Limit: Limit= Limit= Limit= Limit: ALARAGoal= 2.25E-14 uCi/ml ALARA Goal= SE-15 uCi/ml ALARAGoal= 2.25E-l3 uCi/ml ALARA Goal= l.SE-13 uCi/ml ALARA Goal= 1E-15.uCi/ml Pre 1994 MPC SE-12 uCi/ml Pre 1994 MPC SE-14 uCi/ml Pre 1994 MPC 2E-12 uCi/ml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable Limit= Limit= Limit= Limit= Limit= Pre 1994 l.ZSE-12 uCi/ml Pre 1994 SE-13 uCi/ml Pre 1994 A LARA 1E-12 uCi/ml Pre 1994 Not Applicable ALARAGOAL: ALARAGOAL= GOAL= ALARAGOAL= Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 4/3/2006 5.22E-16 9.00E-14 2.25E-14 6.66E-16 2.00E-14 5.00E-15 ;l.llE-16 9.00E-13 ·2.25E-13 9.34E-15 6.00E-13 1.50E-13 Not Analyzed . Not Applicable Not Applicable 7/3/2006 3.08E-16 9.00E-14 2.25E-14 l.lOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.25E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 10/2/2006 9.14E-16 9.00E~14 2.25E-14 4.95E-16 2.00E-14 S.OOE-15 1.86E-16 9.00E-13 2.25E-13 1.67E·14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 1/1/2007 9.49E-16 9.00E-14 2.25E-14 6.81E-16 2.00E-14 S.OOE-15 2.02E-16 9.00E-13 2.25E-13 1.31E·14 6.00E-13 1.50E-13 Not Analyzed Not A~plicable Not Applicable 4/2/2007 l.OSE-15 9.00E-14 2,25E-14. 8.22E·16 2,00E-14 S.OOE-15 2.26E-16 9.00E-13 2.25E-13 1.64E-14 6.00E-13 1.50E-13 f'lot Analyzed Not Applicable Not Applicable 7/2/2007 1.54E-15 9.00E-14 2.25E-14 8.16E·16 2 .. 00E-14 S.OOE-15 4.76E-16 9.00E-13 2.25E-13 2.12E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/30/2007 4.90E-16 9.00E-14 2.25E-14 2.37E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 6.65E-15 6.00E-13 1.50E-13 jllot Analyzed Not Applicable Not ARplicable 12/31/2007 1.46E-15 9.00E-14 2.25E-14 5.67E-16 2.00E-14 S.OOE-15 ,l.OOE-16 9.00E-13 2.25E-13 1.02E·14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not ~plicable 3/31/2008 3.16E-16 9.00E-14 2.25E-14 6.17E·16 2.00E-14 S.OOE-15 3.71E-16 9.00E-13 2.25E-13 4.82E-15 6.00E-13 1.50E-13 Not Anajyzed Not A!lilJicable Not Applicable 6/30/2008 3.13E-15 9.00E-14 2.25E-14 1.55E·15 2.00E-14 S.OOE-15 9.27E-16 9.00E-13 2.25E-13 7.40E-15 6.00E-13 1.50E-13 Not Analyzed Not A~licable Not Applicable 9/30/2008 7.08E-15 9.00E-14 2.25E-14 3.41E-15 2.00E-14 5.00E-15 2.52E-15 9.00E-13 2.25E-13 1.15E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/31/2008 7.22E·15 ·9.00E-14 .2.25E-14 2.82E-15 2.00E-14 5.00E-15 3.03E-15 9.00E-13 2.25E-13. 1.59E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/15/2009 4.13E-15 9.00E-14 2.25E-14 1.39E-15 2.00E-14 5.00E-15 1.41E-15 9.00E-13 2.25E-13 4.66E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/15/2009 2.31E-16 9.00E-14 2.25E-14 7.79E-16 2.00E-14 5.00E-15 6.37E-16 9.00E-13 2.25E-13 4.18E-15 6,00E-13 1,50E-13 Not Analyzed 1 Not Applicable jllot Applicable 9/15/2009 3.10E-15 9.00E-14 2.25E-14 9.20E-16 z.OOE-14 5.00E-15 6.36E-16 9.00E-13 2.25E-13 1.21E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable ,Not Applicable 12/15/2009 5.77E-15 9.00E-14 2.25E-14 3.13E-16 2.00E-14 5.00E-15 1.92E·l6 9.00E-13 2.25E-13 2.48E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/31/2010 4.78E-15 9.00E-14 .2.25E-14 3.73E·16 2.00E-14 5.00E-15 4.19E-16 9.00E-13 2.25E-13 1.30E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2010 4.35E·15 9.00E-14 2.25E-14 7,84E·16 2,00E-14 5.00E-15 1.05E-15 9.00E-13 2.25E-13 4.40E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/30/2010 3.57E-15 9.00E-14 2.25E-14 1.14E·15 2.00E-14 5.00E-15 7.97E-16 g.OOE-13 • 2.25E-13 3.78E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/31/2010 8.52E-15 9.00E-14 2.25E-14 1.45E-15 2.00E-14 5,00E-15 1.29E-15 9.00E-13 ;2.25E-13 1.33E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/4/2011 3.20E-15 9.00E-14 2.25E-14 8.89E-16 2.00E-14 5.00E-15 1.10E-15 9.00E-13 2.25E-13 1.48E·14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/4/2011 6.98E-15 l3.00E-14 2.25E-14 2.03E-15 2.00E-14 5.00E-15 2.52E-15 9.00E-13 2.25E-13 1.08E·14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 10/3/2011 3.11E-15 9.00E-14 'z.25E-14 1.14E·15 2.00E-14 5.00E-15 5.75E·16 9.00E-13 2.25E-13 1.41E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 1/3/2012 4.44E-15 9.00E-14 2.25E-14 2.14E·15 2.00E-14 S.OOE·15 1.53E-15 EJ.OOE-13 2.25E-13 2.05E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/3/2012 5.52E-15 9.00E-14 2.25E-14 3.24E-15 2.00E-14 5.00E-15 1.79E-15 9.00E-13 2.25E-13 1.55E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/2/2012 5.87E-15 9.00E-14 2.25E-14 3.06E·15 2.00E-14 S.OOE-15 1.21E-15 9.00E-13 2.25E-13 1.11E-14 G.OOE-13 L50E-13 Not Analyzed Not Applicable Not Applicable - 10/1/2012 6.73E-15 9.00E-14 2.25E-14 2.59E-15 2.00E-14 S.OOE-15 2.43E-15 9.00E-13 2.25E-13 L30E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/31/2012 4.50E·15 9.00E-14 2.25E-14 1.62E-15 2.00E-14 S.OOE-15 1.79E-15 9.00E-13 2.25E-13 1.74E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable · Not Applicable 3/25/2013 6.66E-15 9.00E-14 2.25E-14 1.48E-15 2.00E-14 5.00E-15 1.12E-15 9.00E-13 2.25E-13 1.80E-14 6.00E-13 1.50E-13 Not Analyzed Not A~licable Not Ap.Qiicable 7/2/2013 7.35E-15 .9.00E-14 2.25E-14 1.72E-15 Z.OOE-14 S.OOE-15 2.02E-15 9.00E-13 2.25E-13 6.67E-15 6.00E-13 1.50E-13 Not Analyzed · Not Applicable Not Applicable 9/30/2013 2.78E-15 ~.OOE-14 2.25E-14 6.92E-16 2.00E-14 S.OOE-15 3.29E-16 9.00E-13 2.25E-13 6.62E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/30/2013 6.70E-15 9.00E-14 2.25E-14 3.93E-16 2.00E-14 5.00E-15 2.53E-16 9.00E-13 2.25E-13 2.78E-14 6.00E-13 l.SOE-13 Not Analyzed ' Not Applicable Not Applicable 3/31/2014 4.74E-15 9.00E-14 2.25E-14 1.42E-15 2.00E-14 S.OOE-15 3.48E-15 9.00E-13 2.25E-13 l.SOE-14 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 6/30/2014 8.18E-15 9.00E-14 2.25E·14 1.34E-15 2.00E-14 S.OOE-15 PGE-15 ll.OOE-13 2.25E-13 1.42E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/30/2014 1.32E-14 9.00E-14 2.25E-14 7.76E-16 2.00E-14 5.00E-15 1.04E-15 9.00E-13 2.25E-13 1.23E·14 6.00E-13 1.50E-13 4.66E-17 4.00E-15 1.00E-15 12/29/2014 S.OOE-16 g.OOE-14 2.25E-14 2.00E-16 2.00E-14 5.00E-15 3.00E-16 9.00E-13 2.25E-13 2.10E-14 6.00E-13 1.50E-13 S.OOE-18 II.OOE-15 1.00E·15 3/30/2015 l.OOE-14 9.00E-14 2.25E-14 S.OOE-16 2.00E-14 5.00E-15 2.10E-15 9.00E-13 2.25E-13 3.10E-14 6.00E-13 1.50E-13 3.00E-18 4.00E-15 l.OOE-15 6/29/2015 4.60E-15 9.00E-14 2.25E-14 S.OOE-16 2.00E-14 5.00E-15 3.70E-15 9.00E-13 2.25E-13 1.40E-14 6.00E-13 1.50E-13 2.00E-17 4.00E-15 l.OOE-15 9/28/2015 1.20E-14 9.00E-14 2.25E-14 ' 4.00E-16 2.00E-14 5.00E-15 9.80E-16 9.00E-13 2.25E-13 1.20E-14 6.00E-13 1.50E-13 'l.OOE-17 4.00E-15 l.OOE-15 12/28/2015 7.40E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.90E-16 EJ.OOE-13 2.25E-13 2.20E-14 6.00E-13 1.50E-13 2.00E-17 4.00E-15 l.OOE-15 3/28/2016 1.40E·15 9.00E-14 2.25E-14 6.00E-16 2.00E-14 5.00E-15 6.20E-15 9.00E-13 2.25E-13 2.30E-14 6.00E-13 1.50E-13 o.OOE-17 II.OOE-15 l.OOE-15 6/27/2016 3.90E-15 9.00E-14 2.25E-14 4.00E-16 2.00E-14 5.00E-15 6,00E-16 9.00E-13 2.25E-13 1.50E-14 6.00E-13 1.50E-13 3.00E-18 4.00E-15 1.00E-15 9/27/2016 7.10E-15 9.00E-14 2.25E-14 7.60E-16 2.00E-14 5.00E-15 1.10E-15 9.00E-13 2.25E-13 2.90E-16 6.00E-13 1.50E-13 3.00E·17 4.00E-15 l.OOE-15 12/27/2016 5.10E·15 9.00E-14 2.25E-14 6.60E-16 2.00E-14 5.00E-15 9.60E-16 9.00E-13 2.25E-13 2.10E-14 G.OOE-13 1,50E·13 ;1.30E-17 4.00E-15 1.00E-15 -:§ 0 j -1/) t: 0 ; ca ... -t: C1) (.) t: 0 0 C1) 'tJ (j j t: .2 'tJ ca a: Ll) > :I: m C\1 ..- I w 0 ~ ..- C') ..- I w 0 ~ '~--~~ ~ lk ~ ·~ ... ... ~ ~ .:; .. ~ , I• :::; ~ .. llo:: f.-~ -~,. ~ 1111 ... ~ le 141 !..4 ~ ~ -:Ji ~~ ~ I ~ ~ !==: ~ .. 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I UJ 0 ~ ..... 9~-das 9~-das 17~-das 8~-das c::~-das ~ ~-das o~-das 6o-das so-das La-das 9o-das so-das 17o-das 8o-das c::o-das ~o-das oo-das 66-das 96-das L6-das 96-das 96-das 176-das 86-das <::6-das ~6-das 06-das 6s-das ss-das La-das 99-das ss-das 179-das E:s-das c::s-das ~s-das Sep-14 Oct-14 Nov-14 Dec-14 Jan-15 Feb-15 Mar-15 Apr-15 May-15 Jun-15 Jul-15 Aug-15 Sep-15 Oct-15 Nov-15 Dec-15 Jan-16 Feb-16 Mar-16 Apr-16 May-16 Jun-16 Jul-16 Aug-16 Sep-16 Oct-16 Nov-16 Dec-16 ..... 0 0 m I ..... co 1/ I \ ·K ..... ..... 0 0 0 0 m m I I ..... ..... -....! O'l ~ I I I 1\ 1/ 1\ \ \ v // "" '\ I J ..... (Log Scale)_. 0 0 0 0 0 0 0 0 m m m m I I I I ..... ..... ..... ..... 01 ~ w 1\) ..... 0 0 r;n ..... :J>m ·= :~>c: ll n> :1>3, G>o 0 0 Ill :::l -0 II 11> ..... ::;, . -o -. m !!l. I -• ....o.o en :;, c r- C') -· -·3 [; .,.. m I ..... (11 c C') ~ m ::I: ~ (11 -t :::r 0 ~­t: 3 I 1\) (A) 1\) 0 0 ::::J () CD ::::J -.., m e. 0 ::::J (/1 -t: 0 ::::::.: 3 - TAB6 BHV-6 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent 9E-14 uCi/ml BHV-6U Effluent ZE-14 uCi/ml BHV-6T230 Effluent 9E-13 uCi/ml BHV-6R Effluent 6E-13 uCi/ml BHV-6PB Effluent 4e-15 uCi/ml BHV-6T232 I Concentration Concentration Concentration Concentration Concentration Pmit= Limit= Limit= limit= Limit= "' AlARAGoal = 2.25E-14 uCi/ml ALARA Goal= SE-13 uCi/ml AlARAGoal = 2.25E-13 uCi/ml ALARAGoal = l .SE-13 uCi/ml }\.LARA Goal= 1E-15 uCi/ml Pre 1994"MPC SE-12 uCi/ml Pre 1994 MPC BE-14 uCi/ml Pre 1994 MPC ZE-12 uCi/ml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable limit= Limit= "!-imit= Limit= Limit= Pre 1994 1.25E-12 uCi/ml Pre 1994 SE-13 uCi/ml Pre 1994 1E-12 uCi/ml Pre 1994 Not Applicable ALARAGOAL= ALARAGOAL= ALARAGOAL= ALARAGOAL= Cone ,EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 5.00E-12 L25E-12 8"00E-14 2.00E-14 Z.OOE-12 5.00E-13 4"00E-12 l.OOE-12 Not Analyzed Not ,o\p_plicable Not Applicable 12/14/1981 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4"00E-12 l.OOE-12 Not AnaJyzed Not Applicable Not Applicable 3/29/1982 5.00E-12 1"25E-12 8.00E-14 2.00E-14 2"00E-12 S.OOE-13 4.00E-12 1"00E-12 Not Analyzed Not Applicable Not Applicable 6/30/1982 5.00E-12 J,.25E-12 8.00E-14 2.00E-14 Z.OOE-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 9/27/1982 S.OOE-12 1.25E-12 8.00E-14 2.00E·14 Z.OOE-12 S.OOE-13 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 1/3/1983 -S.OOE-12 l.ZSE-12 S.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 LOOE-12 Not Analyzed Not Applicable Not Applicable 4/4/1983 -S.OOE-12 l.ZSE-12 S.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed NOt Applicable Not Applicable 6/30/1983 S.OOE-12 1.25E-12J 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 10/3/1983 S"OOE-12 1.25E·12 ROOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 1/3/1984 S.OOE-12 1.25E-12 ROOE-14 2.00E-14 2.00E-12 5"00E-13 4.00E-12 l.OOE-12 Not Analyzed f'lot A_p_plicable Not Applicable 4/2/1984 S"OOE-12 L25E-12 8.00E-14 Z.OOE-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 7/2/1984 5.00E-12 1.25E-12 8.00E-14 Z.OOE-14 Z.OOE-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed 'Not Applicable Not Applicable 10/1/1984 S.OOE-12 1.25E-12 8.00E-14 Z.OOE-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not AppiLcable 1/2/1985 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 4/1/1985 S.OOE-12 l.ZSE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4"00E-12 l.OOE-12 No~ Analyzed Not Applicable Not Applicable 7/1/1985 5.00E-12 l.ZSE-12 8"00E-14 2.00E-14 Z.OOE-12 5.00E-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 9/30/1985 --5.00E-12 1.25E-12 8.00E-14 2"00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable i'Jot Applicable 1/2/1986 5.00E-12 L25E-12 S.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 4/1/1986 5.00E-12 .1.25E-12 8.00E-14 2.00E-14 Z.OOE-12 5.00E-13 4,00E-12 l.OOE-12 Not Analyzed Not Applicable Not A_pplicable 6/30/1986 S.OOE-12 1.25E-12 S.OOE-14 2.00E-14 Z.OOE-12 5.00E-13 4.00E-12 1.00E-1Z Not Analyzed Not Applicable Not Applicable 10/27/1986 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l .OOE-12 Not Analyzed Not Applicable Not Applicable 12/15/1986 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4"00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 3/16/1987 S.OOE-12 1.25E-12 S.OOE-14 2.00E-14 2"00E-12 S.OOE-13 4"00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/11/1987 5.00E-12 1.25E-12 8.00E-14 2"00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 9/9/1987 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/2/1987 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed NOt Applicable Not Applicable 2/16/1988 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/18/1988 S.OOE-12 1.25E-12 8.00E-14 2,00E-14 -2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not 1\llJllicable 8/15/1988 -S.OOE-12 l.ZSE-12 B.OOE-14 2.00E-14 2"00E-12 S.OOE-13 4.00E-12 1"00E-12 Not Analyzed Not Applicable Not Applicable 11/14/1988 S.OOE-12 1.25E-12 8.00E-14 Z.OOE-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 i'Jot Analyzed Not Applicable Not Applicable 2/13/1989 S.OOE-12 l.ZSE-12 8.00E-14 Z.OOE-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/15/1989 5.00E-12 1.25E-12 8.00E-14 Z.OOE-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 8/14/1989 5.00E-12 1.25E-12 8.00E-14 2.00E·14 Z.OOE-12 'S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed ' Not Applicable Not Applicable 11/13/1989 S.OOE-12 1.25E-12 S.OOE-14 Z.OOE-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/12/1990 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 NOt Analyzed Not Applicable Not Applicable 5/14/1990 5.00E-12 1.25E-12 8.00E-14 2"00E-14 2.00E-12 S.OOE-13 4"00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 8/13/1990 5.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 Not Analyzed Not AQplicable Not Applicable 11/12/1990 5.00E-12 L25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/11/1991 5.00E-12 J..25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1,00E-12 Not Analyzed Not Applicable Not Applicable 5/13/1991 5.00E-12 USE-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable ' Not Applicable 8/12/1991 5.00E-12 1.25E-12 8.00E-14 2"00E-14 ~.OOE-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/11/1991 5"00E-12 L25E-12 8.00E-14 2.00E-14 2"00E-12 5.00E-13 4.00E-12 LOOE-12 Not Analyzed Not Applicable NOt Applicable 2/10/1992 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 Not Analyzed Not Applicable Not Applicable 5/11/1992 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 L OOE-12 Not Analyzed Not Applicable Not Applicable 8/10/1992 5.00E-12 L25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 LOOE-12 Not Analyzed Not ARPiicable Not Applicable 11/9/1992 S.OOE-12 L25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/9/1993 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 LOOE-12 Not Analyzed Not Applicable Not Applicable 5/10/1993 5"00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4"00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/10/1993 5.00E-12 1.25E-12 S.OOE-14 2.00E-14 2"00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed ' Not Applicable Not Applicable - Date Effluent 9E-14 uCi/ml BHV-6U Effluent 2E-14 uCi/ml BHV-6T230 Effluent 9E-13 uCi/ml BHV-6R Effluent 6E-13 uCi/ml BHV-6PB Effluent 4e-15 uCi/ml 8HV-6T232 Concentration Concentration Concentration Concentration Concentration Limit= Limit= Limit= Limit= Limit= ALARAGoal = 2.25E-14 uCi/ml ALARA Goal= SE-13 uCi/ml ALARA Goal= 2.25E-13 uCi/ml ALARA Goal= l.SE-13 uCi/ml ALARAGoal-1E-15 uCi/ml Pre 1994 MPC SE-12 uCi/ml Pre 1994 MPC BE-14 uCi/ml Pre 1994 MPC ZE-12 uCi/ml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable Limit= limit= Limit= Limit= Limit= - Pre 1994 1.25E-12 uCi/ml Pre 1994 SE-13 uCi/ml Pre 1994 1E-12 uCi/ml Pre 1994 Not Applicable ALARAGOAL= ALARAGOAL= ALARAGOAL= ALARAGOAL= Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC -EFCA 11/8/1993 S.OOE-12 1.25E-12 8.00E-14 .2-00E-14 2.00E-12 &.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/7/1994 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2_00E-12 S.OOE-13 4-00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 5/9/1994 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2_00E-12 .S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 8/9/1994 S_OOE-12 1.25E-12 8.00E-14 2-00E·14 2.00E-12 5-00E-13 4_00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 11/7/1994 !i-OOE-12 1.25E-12 8.00E-14 2_0QE-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 Not Analyzed Not Applicable Not Applicable 2/7/1995 ':J_QOE-14 2.25E-14 2.00E-14 S_OQE-15 9.00E-13 1.25E-13 6.00E-13 1.50E-13 NOt Analyzed Not Applicable Not Applicable 5/9/1995 g_QOE-14 2.25E-14 2_0QE-14 5.00E-15 g_OOE-13 1.25E-13 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 8/9/1995 9-00E-14 2.25E-14 2_QOE-14 5.00E-15 9_00E-13 2.25E-13 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 11/11/1995 9-00E-14 2-25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6-00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 2/5/1996 v 9_00E-14 2.25E-14 2.00E-14 5_00E-15 9.00E-13 2.25E-13 6.00E-13 1-SOE-13 Not Analyzed Not Appjicable Not Applicable 5/6/1996 9.00E-14 2-25E-14 l .OOE-14 5_00E-15 9.00E-13 2.25E-13 6.00E-13 L50E-13 Not Analyzed Not Applicable Not Applicable 8/5/1996 9_00E-14 2-2SE-14 z_ooe-14 5.00E-15 9-00E-13 2.25E-13 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 11/6/1996 9_00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6_00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 2/6/1997 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6_00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 5/5/1997 9.00E-14 2.25E-14 2-00E-14 S_OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 8/11/1997 9.00E-14 2.25E-14 Z.OOE-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 1/5/1998 9-00E-14 2.25E-14 2.00E-14 5_00E-15 9_00E-13 2-25E-13 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/28/1998 9_00E-14 2.2SE-14 2,00E-14 5.00E-15 9.00E-13 2.25E-13 6_00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/31/1998 9.00E-14 2.25E-14 2.00E-14 5-00E-15 9.00E-13 2.25E-13 6_00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/28/1998 9.00E-14 2.25E-14 2.00E-14 5-00E-15 9_00E-13 2.25E-13 6_00E-13 1.50E-13 Not Analyzed Not Applicable _ Not Ap!1!icable 12/28/1998 9.00E-14 2-ZSE-14 l _OOE-14 5.00E-15 9_00E-13 2.25E-13 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/29/1999 9_00E-14 2.25E-14 2.00E-14 s_ooE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/3/1999 9.00E-14 2-25E-14 2-00E-14 5,00E·15 9.00E-13 2-25E-13 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/27/1999 3.03E-15 9_00E-14 2-25E-14 1.37E-15 2.00E-14 5_00E-15 8.72E-16 9_00E-13 2.25E-13 7.55E-15 6_00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/28/1999 5.01E-15 • 9_00E-14 2.25E-14 2.89E-15 2 .. 00E-14 S.OOE-15 l.31E-15 ROOE-13 .2.25E-13 8.10E-15 6_00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/30/2000 7.46E-16 9.00E-14 2-25E-14 5.25E-16 2.00E-14 S_OOE-15 3.00E-16 S.OOE-13 .2.25E-13 7.83E-15 6_QQE-13 1.50E-13 NOt Analyzed Not Applicable Not Applicable 6/26/2000 5.40E-16 9.00E-14 2-25E-14 3-53E-16 2.00E-14 s_ooE-15 6.11E-16 9_00E-13 l .25E-13 4_83E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/25/2000 3_75E-16 9_00E-14 2-25E-14 2BE-16 zmE-14 5.00E-15 1.91E-16 g_ooE-13 2.25E-13 6.41E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/26/2000 5.21E-16 9_00E-14 2.25E-14 3.39E-16 l_QOE-14 5.00E-15 3_28E-17 g_ooE-13 l .25E-13 8.57E-15 6_QOE-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/26/2001 1.4lE-16 9_00E-14 2.ZSE-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9-00E-13 2.25E-13 6.15E-15 6-00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/2/2001 1.81E-16 9_00E-14 :z.z5E-14 1.66E-16 2.00E-14 5_00E-15 l.OOE-16 9_00E-13 2.25E-13 6_95E-15 6_00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/24/2001 3_08E-16 9.00E-14 :Z.2SE-14 1.01E-16 2.00E-14 5_00E-15 L77E-16 9.00E-13 2.25E-13 8.59E-15 6_00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/31/2001 3_31E-16 9-00E-14 :Z.25E-14 1.25E-16 2.00E-14 5_0QE-15 1.09E-16 9.00E-13 .2.25E-13 3-14E-15 6_00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/1/2002 4.77E-16 9.00E-14 l1-25E-14 z_94E-16 2.00E-14 5_00E-15 1.96E-16 9_00E-13 2.25E-13 8_61E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/1/2002 3-68E-16 9.00E-14 2.25E-14 4.41E-16 2.00E-14 5.00E-15 1.76E-16 9_00E-13 2-25E-13 8.20E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/30/2002 3_67E-16 9.00E-14 2-25E-14 5,60E-16 2_00E-14 5.00E-15 1.80E-16 9_00E-13 2.25E-13 5.55E-15 6.00E-13 1.SOE-13 Not Analyzed Not Applicable Not Applicable 12/30/2002 LOOE-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 1.67E-16 9_00E-13 2.25E-13 1.35E-14 6-00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/31/2003 1.98E-16 9-00E-14 2.25E-14 1.68E-16 2.00E-14 5-00E-15 1.00E-16 ~.OOE-13 2.25E-13 7_77E-15 6_00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2003 l .18E-16 9.00E-14 2.25E-14 U5E-16 2.00E-14 5-00E-15 LOOE-16 9.00E-13 2.25E-13 5.92E-15 6_00E-13 L50E-13 Not Analyzed Not Applicable Not Applicable 9/29/2003 LOOE-16 9_00E-14 2.25E-14 LOOE-16 2_00E-14 s_ooE-15 LOOE-16 9_00E-13 2.25E-13 B-30E-15 6.00E-13 L50E-13 Not Analyzed Not Applicable Not Applicable 12/29/2003 LOOE-16 jl.OOE-14 2-25E-14 L36E-16 2_00E-14 s_ooE-15 l.OOE-16 9-00E-13 2,25E-13 6_66E-15 6.00E-13 L50E-13 Not Analyzed Not Applicable Not Applicable 3/29/2004 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2-00E-14 5,00E-15 l.OOE-16 9_00E-13 2.25E-13 8.17E-15 6.00E-13 1.50E-13 Not Analyzed NOt Applicable Not Applicable 6/27/2004 LOOE-16 9-00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.00E-16 9_00E-13 2_25E-13 3.55E-15 6.00E-13 l.SOE-13 Not Analyzed Not Applicable Not Applicable 9/27/2004 LOOE-16 9-00E-14 2.25E-14 1.38E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2-25E-13 1.22E-14 6-00E-13 L50E-13 Not Analyzed Not Applicable Not Applicable 12/27/2004 L05E-16 9_QOE-14 2.25E-14 1.72E-16 2.00E-14 5-00E-15 LOOE-16 9.00E-13 2.25E-13 1.52E-14 6.00E-13 L50E-13 Not Analyzed Not Applicable Not Applicable 3/28/2005 LOOE-16 B.OOE-14 2.25E-14 LOOE-16 2.00E-14 S_OOE-15 l.OOE-16 9_00E-13 2.25E-13 9_34E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/29/2005 L28E-16 .9.00E-14 2.25E-14 L01E-16 2.00E-14 s_ooE-15 l.OOE-16 9_0QE-13 2.25E-13 g_8sE-15 6.00E-13 L50E-13 Not Analyzed Not Applicable Not Applicable 9/26/2005 L98E-16 9.00E-14 2,25E-14 5.98E-16 2.00E-14 S.OOE-15 :0t55E-16 9_00E-13 2.25E-13 1.71E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 1}3/2006 7_67E-16 , 9-00E-14 2.25E-14 2.88E-16 2_00E-14 S.OOE-15 3_60E-l5 9.00E-13 2.25E-13 4.85E-14 6.00E-13 1.SOE-13 Not Analyzed Not Applicable Not Applicable Oate Effluent 9E-14 uCi/ml BHV-6U Effluent 2E-14 uCi/ml BHV-6T230 Effluent 9E-13 uCi/ml BHV-6R Effluent 6E-13 uCi/ml BHV-6PB Effluent 4e-15 uCi/ml BHV-6T232 toncentration Concentration Concentration Concentration Concentration Limit= Limit= Limit= limit= Limit= ALARAGoal= 2.25E-14 uCi/ml ALARA Goal= SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml ALARAGoal = 1E-15 uCi/ml Pre 1994 MPC SE-UuCi/ml Pre 1994 MPC SE-14 uCi/ml Pre 1994 MPC ZE-12 ucirml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable Limit= Limit= Limit= Limit= Limit= 'Pre 1994 1.25E-12 uCi/ml Pre 1994 SE-13 uCi/ml Pre 1994 1E-12 uCi/ml Pre 1994 Not Applicable ALARAGOAL= ALARAGOAL= ALARAGOAL= ALARAGOAL= (one EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone ~FC EFCA 4/3/2006 2.92E-16 9.00E-14 2.25E-14 2.00E-16 2.00E-14 S.OOE-15 l.OOE-16 ~.OOE-13 2,25E-13 1.11E-14 6.00E-13 1.50E-13 f'lot Analyzed Not 1\ru>licable Not Ap~licable 7/3/2006 3.25E-16 9.00E-14 2.25E-14' ;!.36E-16 2.00E-14 5.00E-15 l.OSE-16 B.OOE-13 2.25E-13 1.10E-14 6.00E-13 1.50E-13 Not Analyzed Not ~plicable Not Applicable 10/2/2006 5.03E-16 9.00E-14 2.25E-14 1.49E-16 2.00E-14 S.OOE-15 1.19E-16 B.OOE-13 2.25E-13 2.13E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable 'Not Applicable 1/1/2007 8.31E-16 9.00E-14 , 2.25E-14 2.49E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.70E·14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Appjicable 4/2/2007 5.36E-16 9.00E-14 2.25E-14 3.15E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E·13 2.25E-13 1.43E·14 6.00E·13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/2/2007 1.08E·l5 9.00E-14 2.25E-14. 2.18E·16 2.00E·14 5.00E-15 1.54E·16 9.00E·13 2.25E-13 2.04E·14 G.OOE-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/30/2007 3.92E·16 9.00E-14 2.25E·14 1.02E·16 .l.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E·13 6.38E·15 6.00E-13 1.50E·13 Not Analyzed Not Applicable f'lot Applicable 12/31/2007 2.92E·l5 9.00E-14 '2.25E-14 1.55E·15 2.00E-14 5.00E-15 3.16E·16 9.00E-13 2.25E-13 9.19E-15 G,OOE-13 1,50E-13 Not Analyzed Not Applicable f'lot Applicable 3/31/2008 4.34E-16 9.00E-14 2.25E-14 3.51E-16 2.00E-14 5.00E·15 l.OOE-16 9.00E-13 2.25E-13 5.99E-15 6.00E-13 1.50E·13 Not Analyzed Not Applicable Not Applicable 6/3102008 1.88E-15 9.00E-14 2.25E-14 9.00E-16 2.00E-14 5.00E-15 4.04E-16 9.00E-13 2.25E-13 7.41E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/30/2008 4.82E·15 9.00E-14 : 2.25E-14 2.10E-15 2.00E-14 5.00E-15 1.27E-15 9.00E-13 2.25E-13 l.OOE-14 6.00E·13 1.50E-13 Not Analyzed Not Applicable Not AJlplicable 12/31/2008 4.80E-15 9.00E-14 2.25E-14 1.70E-15 2.00E-14 5,00E-15 1.25E·15 9.00E-13 2.25E-13 1.49E·14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/15/2009 2.77E-15 9.00E-14 2.25E-14 1.01E-15 2.00E-14 5.00E·15 7.82E-16 9.00E-13 2.25E-13 6.46E-15 6.00E-13 1.50E·13 Not Analyzed Not Applicable Not Applicable 6/15/2009 1.41E-16 9.00E-14 2.25E-14 2.67E-16 2.00E-14 5.00E-15 1.81E-16 9.00E-13 2.25E-13 5.76E·15 6.00E-13 1.50E-13 Not Analyzed f'lot Applicable Not Applicable 9/15/2009 4.87E-15 9.00E-14 2.25E-14 4.32E·16 2.00E·14 5.00E-15 2.23E-16 9.00E·13 2.25E-13 8.98E·15 6,00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/15/2009 9.24E-15 9.00E-14 2.25E-14 2.26E·16 2.00E-14 5.00E-15 1.15E·16 9.00E-13 2.25E-13 6.44E·15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/31/2010 9.63E-15 9.00E-14 2.25E-14 1.82E-16 2.00E-14 5.00E-15 2.06E·16 9.00E-13 2.25E·13 1.37E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2010 3.62E·15 9.00E·14 .2.25E-14 3.94E-16 2.00E-14 5.00E-15 4.89E-16 9.00E-13 2.25E-13 4.30E-15 6.00E·13 1.50E-13 Not Analyzed Not Applicable Not Applicable 9/30/2010 5.42E-15 9.00E·14 2.25E-14 1.08E·15 2.00E-14 5.00E-15 5.68E-16 9.00E-13 2.25E-13 3.98E·15 6.00E-13 1.50E-13 Not Analyzed f'lot Applicable Not Applicable 12/31/2010 1.24E·14 9.00E-14 2.25E-14 1.21E·15 2.00E-14 5.00E-15 1.00E·15 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/4/2011 2.70E·15 9.00E·14 2.25E-14 4.62E·16 2.00E·14 5.00E-15 6.51E-16 9.00E-13 2.25E-13 1.29E·14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/4/2011 3.01E-15 g.OOE-14 ·2.25E-14 7.07E-16 2.00E-14 5.00E-15 5.75E-16 9.00E-13 2.25E-13 7.97E-15 6.00E-13 1.50E-13 Not Analyzed ~ot Applicable Not Applicable 10/3/2011 2.05E-15 9.00E-14 2.25E-14 6.12E-16 2.00E-14 5.00E-15 l.SSE-16 9.00E-13 2.25E-13 9.93E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 1/3/2012 3.14E-15 9.00E-14 2.25E-14 1.09E-15 2.00E-14 5.00E-15 7.65E-16 9.00E-13 2.25E-13 1.89E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 4/3/2012 4.41E-15 9.00E-14 2.25E-14 1.82E-15 2.00E·14 S.OOE-15 II.OOE-16 9.00E-13 2.25E-13 1.50E-14 6,00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 7/2/2012 6.42E·15 "9.00E-14 2.25E-14 2.25E-15 2.00E-14 5.00E-15 •S.llE-16 9.00E-13 2.25E-13 9.54E-15 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 10/1/2012 6.63E-15 9.00E-14 2,25E-14 1.31E·15 2.00E-14 5.00E-15 1.22E-15 9.00E-13 2.25E-13 1.34E·14 6,00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 12/31/2012 3.83E-15 9.00E-14 2.25E-14 1.18E-15 2.00E-14 S.OOE-15 9.30E·16 9.00E-13 2.25E-13 1.60E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/25/2013 4.52E-15 9.00E-14 2.25E-14 7.93E·16 2.00E-14 5.00E-15 4.91E-16 9.00E-13 2.25E-13 1.70E-14 6.00E-13 1.50E-13 Not Analyzed ,Not Applicable Not Applicable 7/2/2013 5.91E-15 9.00E-14 2,25E-14 6.74E·16 2.00E-14 S.OOE-15 7.85E-16 9.00E-13 2.25E-13 5.18E·15 6.00E-13 1.50E-13 Not Analyzed Not ,6,pplicable Not Applicable 9/30/2013 2.68E·15 9.00E-14 2.25E-14 3.97E-16 2.00E-14 5.00E-15 1.04E·16 9.00E-13 2.25E-13 6.13E·15 6.00E·l3 l.SOE-13 Not Analyzed Not Applicable Not Applicable 12/30/2013 1.60E-14 9.00E-14 2.25E-14 2.48E·l6 2.00E-14 5.00E-15 1.05E·16 9.00E-13 2.25E-13 2.67E·14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 3/31/2014 8.92E-15 9.00E-14 2.25E-14 7.68E-16 2.00E-14 5.00E-15 l.SOE-15 9.00E·13 2.25E-13 1.61E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable 6/30/2014 8.29E-15 9.00E-14 2.25E-14 5.35E-16 2.00E·14 5.00E-15 6.72E-16 9.00E-13 2.25E-13 1.20E-14 6.00E-13 1.50E-13 Not Analyzed Not Applicable Not Applicable S/30/2014 1.20E-14 9.00E-14 2.25E-14 5.54E-16 2.00E-14 5.00E-15 6.18E-16 9.00E·13 2.25E·13 1.38E-14 6.00E-13 1.50E-13 l.OOE-16 4.00E-15 l.OOE-15 12/29/2014 S.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 . 2.25E-13 2.30E-14 6,00E-13 1.50E-13 S.OOE-18 4.00E-15 l.OOE-15 3/30/2015 2.80E-14 s.OOE-14 2.25E-14 2.00E-16 2.00E-14 S.OOE-15 4.00E-16 9.00E-13 ' 2,25E-13 2.80E-14 6.00E-13 1.50E-13 l.OOE-18 4.00E-15 l.OOE-15 6/29/2015 5.30E-15 9.00E-14 2.25E-14 2.00E-16 2.00E-14 5.00E-15 S.OOE-16 9.00E-13 2.25E-13 1.70E-14 6.00E-13 1.50E-13 1.00E-17 4.00E-15 l.OOE-15 9/28/2015 1.00E·14 9.00E-14 2.25E-14 2.00E-16 2.00E-14 5.00E-15 3.00E-16 9.00E-13 2.25E·13 1.10E-14 6.00E-13 1.50E-13 2.00E·18 4.00E-15 l.OOE-15 12/28/2015 :8.40E-16 9.00E-14 2.25E-14 1.00E·16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 2.00E-14 6.00E-13 1,50E-13 6.00E-18 4.00E-15 1.00E-15 3/28/2016 7.00E-16 9.00E-14 2.2SE·14 l.OOE-16 2.00E-14 5,00E-15 9,00E·16 9.00E·13 2.25E-13 1.70E-14 6.00E-13 1,50E-13 1.00E-17 4.00E-15 1.,00E-15 6/27/2016 1.20E·14 9.00E-14 2.25E-14 1.00E·16 2.00E-14 5,00E-15 6.00E·l5 9.00E-13 2.25E-13 2.10E·14 6.00E-13 1.50E-13 4.00E·18 4.00E-15 l.OOE-15 9/27/2016 6.90E·15 9.00E-14 2.25E-14 4.00E·16 2.00E-14 S,OOE-15 7.20E-16 9.00E-13 2.2SE·13 3.20E·l5 6.00E·13 l.SOE-13 1.20E·17 4,00E-15 l.OOE-15 12/27/2016 8.90E-15 9.00E-14 2.2SE-14 3.30E·16 2.00E·14 5.00E-15 4.80E-16 9 OOE-13 2.25E-13 2.10E·14 G.OOE-13 1.50E-13 9.50E-18 4.00E·15 l.OOE-15 -- - 9/28/1981 4/4/1983 10/1/1984 4/1/1986 9/9/1987 ±2/13/1989 @ :::::! c:· 8/13/1990 3 z a211o11992 c @ -8/10/1993 + 2/7/1995 -I ::::; g_ 8/5/1996 c 3 ~4/28/1998 0 9/27/1999 t 3/26/2001 ll> c. ~-9/30/2002 !\:, ~3/29/2004 + 9/26/2005 ill 4/2/2007 c. ~9/30/2008 + 3/31/2010 ;! 1 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N 0 0 :J (') CD :J -.., ~ 0 :J C/1 -c 0 ~ ~ TAB7 BHV-7 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent 9E-14 uCi/ml BHV-7U Effluent 2E-14 uCi/ml BHV-7T230 Effluent 9E-13 uCi/ml BHV-7R Effluent 6E-13 uCi/ml BHV-7PB -Effluent 4e-15 uCi/ml BHV-7T232 Concentration Concentration Concentration Concentration Concentration Umit= limit= Umit= limit= limit= ALARAGoal= 2.25E-14 uCi/ml AlARAGoal= SE-13 uCi/ml AlARAGoal = 2.25E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml AlARAGoal-1E-15 uCi/ml Pre1994MPC 5E-12 uCi/ml Pre 1994 MPC SE-14 uCi/ml Pre 1994 MPC 2E-12 uCi/ml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable limit= limit= limit= limit= limit= ' Pre 1994 1.25E-12 uCi/ml Pre 1994 SE-13 uCi/ml Pre 1994 lE-12 uCi/ml 'Pre 1994 Not Applicable ALARAGOAL= ALARAGOAl= AlARAGOAl= ALARAGOAl= Cone 'EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 12/29/2014 NS 9.00E-14 :2.25E-14 NS 2.00E-14 5.00E-15 NS '9.00E-13 2.25E-13 NS G.OOE-13 1.50E-13 NS 4.00E-15 l.OOE-15 -3/30/2015 6.00E-15 9.00E-14 ;l.25E-14 S.OOE-17 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 2.50E-14 6.00E-13 1.SOE-13 7.00E-18 4.00E-15 l.OOE-15 6/29/2015 1.40E-15 '9.00E-14 2.25E-14 4.00E-16 2.00E-14 5.00E-15 1.30E-15 9.00E-13 2.25E-13 1.70E-14 6.00E-13 1.50E-13 1.00E-17 4.00E-15 l.OOE-15 9/28/2015 4.20E-15 9.00E-14 2.25E-14 2.00E-16 2.00E-14 5.00E-15 4.00E-16 9.00E-13 2.25E-13 1.00E-14 6.00E-13 1.50E-13 6.00E-18 4.00E-15 l.OOE-15 12/28/2015 3.60E-16 9.00E-14 2.25E-14 7.00E-17 2.00E-14 5.00E-15 2.00E-16 9.00E-13 2.25E-13 2.00E-14 6.00E-13 1.50E-13 3.00E-18 4.00E-15 l.OOE-15 3/28/2016 B.OOE-16 9.00E-14 .2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-15 9.00E-13 2.25E-13 1.70E-14 6.00E-13 1.50E-13 5.00E-18 4.00E-15 l.OOE-15 6/27/2016 l.SOE-15 9.00E-14 '2.25E-14. 9.00E-17 2.00E-14 5.00E-15 9.00E-16 9.00E-13 2.25E-13 1.50E-14 6.00E-13 1.50E-13 3.00E-18 4.00E-15 l.OOE-15 9/27/2016 2.60E-15 9.00E-14 ;l.25E-14 1.70E-16 2.00E-14 5.00E-15 4,10E-16 9.00E-13 2.25E-13 2.80E-15 6.00E-13 1.50E-13 5.50E-18 4.00E-15 l.OOE-15 12/27/2016 1.60E-15 9.00E-14 ~.25E-14 1.20E-16 2.00E-14 5.00E-15 2.50E-16 9.00E-13 2.25E-13 1.50E-14 G,OOE-13 1.50E-13 4.80E-18 4.00E-15 l.OOE-15 Ul c 0 ·~ ... -c Cl) (,) c 0 0 Cl) :2 0 ::::J c 0 :a ~ a: "" :> :I: m C\J ..... I w 0 ~ ..... \ ( 4 \ lj (t) """ ..... ..... I I w w 0 0 ~ ~ ..... ..... I! r \ I I \~ ~ I \ I ~ i\ 1\ \ .\ ~~ I / ~v v I \ v I ~ ~ I \ v j\~ \ / " I L{) ..... I w 0 ~ ..... (are::>s 6o1) T I~ \ \ I ~ \ I 1/ 4 ~ co ,..... ..... ..... I I w w 0 0 ~ ~ ..... ..... 1\ 1/ 1\ 1/ ..... w 0 ~ ..... C\J (t) C\J E: 9 ~Oc/6c/6 ·E 0 ..c. I- t 0 ..... 9~0G/6G/9C';J -g Q) ....J + co 9Wc/6G/8~ E: :l 'g a: + SWG/6G/G~ 0 (t) C\J E: :l ·;;:: 0 ..c. I- SWG/6G/6 + S~OG/6G/8 1.00E-11 1.00E-12 1.00E-13 Q) (ij ~.OOE-14 0> 0 _J - 1.00E-15 1.00E-16 1.00E-17 -.:t ..... ' (.) Q) 0 Effluent Concentration Limit= 9E-14 uCi/ml ALARA Goal= 2.25E-14 uCi/ml Pre 1994 MPC Limit= 5E-12uCi/ml Pre 1994 ALARA Goal= 1.25E-12 uCi/ml ..... ........... ......... " ........... ~ ~ LO LO LO LO ..... ...-..... ..... .0 ' ' 0, "-c:: Q) c.. ::::J ::::J LL <( ...., <( "' BHV-7 Uranium-Natural Concentrations (uCi/ml) ...... -- ""' _____..--~ -~ -... LO LO <0 <0 <0 <0 <0 ..... ...-..... ..... ..... ..... ..... ' c) ' ' ' 0, ' -.0 .... c:: t5 (.) Q) Q) c.. ::::J ::::J 0 0 LL <( ...., <( 0 1/) c 0 i lo.. -c Cl) u c 0 0 0 (") ~ E ::::J 'i: 0 .c I- " :> :I: m T""" w 0 0 C\1 T""" I w 0 C! C') ~ 10 T""" T""" .-I I I w w w 0 0 0 C! 0 C! (are~s Bol) T I~ \ g~-6nv 9~-unr . 9 ~-qa.:J I I 9~-Bnv IJ 1\ 9~-unr 1\ 1\ ' v~-~aa co 1'-.- I w w 0 0 C! C! 1.00E-11 1.00E-12 1.00E-13 a> Cil ~.OOE-14 0> 0 ....J ~ 1.00E-15 1.00E-16 1.00E-17 -.:t ..... I u <I> 0 Effluent Concentration Limit= 9E-13 uCi/ml ALARA Goal= 2.25E-13 uCi/ml Pre 1994 MPC Limit= 2E-12uCilml Pre 1994 ALARA Goal= SE-13 uCi/ml Ll) ..... I .0 <I> u_ / / / Ll) ..... ~ c.. <( / ~ Ll) ..... I c :::1 ...., Ll) ..... I 0> :::1 <( ......... ~-- Ll) ..... I 0 0 BHV-7 Radium-226 Concentrations (uCi/ml) ----./ Ll) u <I> 0 / ./ c.o ..... .0 <I> u_ c.o ..-1 .... c.. <( c.o ..- 1 c :::1 ...., c.o ..-1 0> :::1 <( ---- ' c.o ..-1 0 0 ~ I 1.00E-11 1.00E-12 1.00E-13 Q) <il (.) C!.I.OOE-14 Cl 0 ::::!- 1.00E-15 1.00E-16 1.00E-17 - - '<t ,..- ' (.) Q) Cl Effluent Concentration Limit= SE-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml Pre 1994 MPC Limit= 4E-12uCi/ml Pre 1994 ALARA Goal = 1 E-12 uCi/ml ~ -..._______ 1.0 ,..- i:J Q) LL. ' 1.0 ,..- ' ..... c. <( 1.0 ,..- ' c: ::I """') 1.0 ,..- ' Cl ::I <( BHV-7 Lead-210 Concentrations (uCi/ml) ------ 1.0 1.0 <D ,..-,..-,..- i:J Q) LL. ' t5 0 ' (.) Q) Cl <D ,..- ' ..... c. <( ~ ,..- C: ::I --, .......... 0, ::I <( ............ / .. ,..- ' -(.) 0 L In c 0 ~ -c Cl) u c 0 0 C\1 C") ~ E j "i: 0 .c 1- r--. > J: al :g (3 :::J ll) .... I w o:t 11 - .'!:: E .§() ...I :::J C::ll) 0 .- ·-I .... w l!!o ..... c::.-~ II §IU o& 'E c:t CII CJ: 2 < :I= ...I W <t C\1 C') "¢ ..... ..-w I w UJ 0 0 0 0 <:! <:! ..-,.... 9~-lOQ 1\ g~-6nv 1\ g ~-unr 1/ g~-qa.:J 1\ • 9~-oaa 1/ 9 ~-lOQ 9 ~-5nv • 9 ~-unr . v ~-oaa I!) co I'-c:o 0) ..-,.... ,.... I w I UJ UJ w I UJ 0 0 0 0 0 0 0 <:! ~(are~s 6o1f ,.... <:! <:! ..-,.... TABS BHV -8 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent 9E-14 uCi/ml BHV-SU Effluent 2E-14 uCi/ml BHV-8T230 Effluent 9E-13 uCi/ml BHV-SR Effluent 6E-13 uCi/ml BHV-SPB ·effluent 4e-15 uCi/ml BHV-8T232 Concentration Concentration Concentration Concentration Concentration Umlt~ Limit= Umlt= Limit= Umit= ALARAGoala 2.25E-14 uCi/ml ALARA Goal-SE-13 uCi/ml ALARAGoal-2.25E-13 uCi/ml ALARA Goal-1.5E-13 uCi/ml ALARAGoal-1E-15 uCi/ml 'i>re 1994 MPC SE-12 uCi/ml Pre 1994 MPC SE-14 uCi/ml Pre 1994 MPC 2E-12 uCi/ml Pre 1994 MPC 4E-12 uCi/ml Pre 1994 MPC Not Applicable J,imit= Limit= Umlt= limit= Limit= Prel994 1.25E-12 uCi/ml Pre 1994 5E-13 uCi/ml Pre 1994 lE-12 uCi/ml Pre 1994 Not Applicable ALARAGOAL~ ALARAGOAL= ALARAGOAL= ALARAGOAL= Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone .EFC EFCA - 12/29/2014 4.00E-16 9.00E-14 2.25E-14 2.00E-16 2.00E-14 5.00E-15 7.00E-17 9.00E-13 2.25E-13 9.90E-15 6.00E-13 1.50E-13 9.00E-18 4.00E-15 1.00E-15 3/30/2015 l.SOE-15 9.00E-14 2.25E-14 4.00E-17 2.00E-14 5.00E-15 4.00E-17 S.OOE-13 2.25E-13 9.40E-15 6.00E-13 1.50E-13 l.OOE-16 4.00E-15 l.OOE-15 6/29/2015 5.00E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 S.OOE-16 9.00E-13 2.25E-13 9.00E-15 6.00E-13 1.50E-13 7.00E-18 4.00E-15 l.OOE-15 9/28/2015 1.80E-15 9.00E-14 2.25E-14 4.00E-17 2.00E-14 5.00E-15 4.00E-16 9.00E-13 2.25E-13 8.00E-15 6.00E-13 1.50E-13 3.00E-18 4.00E-15 l.OOE-15 12/28/2015 2.10E-16 9.00E-14 2.25E-14 9.00E-17 2.00E-14 5,00E-15 9.00E-16 9.00E-13 2.25E-13 2.00E-14 6.00E-13 l.SOE-13 4.00E-18 4.00E-15 l.OOE-15 3/28/2016 2.00E-16 9.00E-14 2.25E-14 2.00E-17 2.00E-14 5.00E-15 3.00E-16 9.00E-13 2.25E-13 1.60E-14 6.00E-13 1.50E-13 2.00E-18 4.00E-15 l.OOE-15 6/27/2016 t.lOE-15 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.90E-15 9.00E-13 2.25E-13 1.10E-14 6.00E-13 l.SOE-13 2.00E-18 4.00E-15 '1.00E-15 9/27/2016 1.20E-15 9.00E-14 2.25E-14 8.40E-17 2.00E-14 S.OOE-15 3.30E-16 9.00E-13 2.25E-13 7.60E-15 6.00E-13 1.50E-13 4.70E-18 4.00E-15 1.00E-15 12/27/2016 1.20E-15 9.00E-14 2.25E-14 6.00E-17 2.00E-14 5.00E-15 8.50E-17 9.00E-13 2.25E-13 1.40E-14 6.00E-13 1.50E-13 3.20E-18 4.00E-15 1.00E-15 en c 0 ·.;; "' .... -c C1) (.) c 0 () C1) :'2 (.) ~ c .2 'tJ "' a: ()C) :> ::I: m C\J C') .-.- I I w w 0 0 '=! '=! .-.- \ 1 ~ \ -.:!" .-I w 0 '=! v ~ IJ ~ 1\ 1\\ \ \ / 1/ I .I K \ 1\ Ur-i\ 1'\ 1\ L{) .-I w 0 '=! .- ( are:>s 1301) I/ ~ ~ f\ "'~ 1/ v ) ~ v v ~ !1[/ 1/ "I\ !'\ v "" CD 1'-.-.-I w w 0 0 '=! '=! .- 1/ 1\ I ~ 1/ v 1\ 1/ co .-w 0 0 0 9~0G/08/9~ -g Q) -1 9WG/08/v + CD C\J C\J E: 9 ~0G/6G/G :6 ell a: + 0 C') C\J E: :::l 9WG/~8/0~ I- t 9 ~0GH8/9Cil .... :::l -ell z E 9 ~OG/08/9 ·~ ~ :::> + 9~0G!O£/v 9~0G/9G/G v~OG/6G/G~ 1.00E-11 1.00E-12 1.00E-13 Q) (il (.) CJ1.00E-1 4 C> ~ 1.00E-15 1.00E-16 1.00E-17 / - -.:t ..- ' (.) Q) 0 Effluent Concentration Limit= 9E-14 uCi/ml ALARA Goal= 2.25E-14 uCi/ml Pre 1994 MPC Limit= 5E-12uCi/ml Pre 1994 ALARA Goal= 1.25E-12 uCi/ml ~ ~ ' LO LO LO LO ..-..-..-..- .iJ ' ' ' .... c Ol Q) a. :::J :::J u. <( """') <( BHV-8 Uranium-Natural Concentrations (uCi/ml) " / ........ / "'-..... / LO LO <D <D <D <D <D ..-..-..-..-..-..-..-' u ' ' C: c, ' t3 .0 .... t3 Q) Q) a. :::J :::J 0 0 u. <( """') <( 0 1.00E-11 1.00E-12 1.00E-13 Q) til (.) C!.I.OOE-14 Cl 0 2- 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit= 2E-14 uCi/ml ALARA Goal= 5E-15 uCi/ml Pre 1994 MPC Limit= 8E-14uCi/ml ~ ""'" ,.... I (.) Q) 0 1.0 ,.... .0 Q) LL ......__ ' 1.0 ,.... ~ c. <{ ' 1.0 ,.... I c ::::J -, 1.0 ,.... I Cl ::::J <{ -- ' 1.0 ,.... I t5 0 BHV-8 Thorium-230 Concentrations (uCi/ml) 1.0 ,.... I (.) Q) 0 ........ .......... ......................... <0 ,.... .0 Q) LL ./"" ,.... ~ c. <{ / c ::::J -, ,.... 0, ::::J <{ ,.... I t5 0 1.00E-11 1.00E-12 1.00E-13 Q) (ij c5l.ooE-14 Cl 0 _J - 1.00E-15 1.00E-16 1.00E-17 - 'o;t ,..... u (J.) Cl Effluent Concentration Limit= 9E-13 uCi/ml ALARA Goal= 2.25E-13 uCi/ml Pre 1994 MPC Limit= 2E-12uCi/ml Pre 1994 ALARA Goal= SE-13 uCi/ml -- / / / -,/ ' ' LO LO LO LO ,..... ,..... ,..... ,..... ' .0 (J.) u.. ' c I ...... Cl 0.. ::I ::I <( """'J <( ~ BHV-8 Radium-226 Concentrations (uCi/ml) ~ I ........ / ........ ........... / ....... I ............ ~ I I LO LO c.o c.o c.o c.o c.o ,..... ,..... ,..... ,..... ,..... ,..... ,..... I I I I I 6l I t5 (.) .0 ...... c -(J.) (J.) 0.. ::I ::I (.) 0 Cl u.. <( """'J <( 0 1.00E-11 1.00E-12 1.00E-13 Q) tti (.) Cf.I.OOE-14 Ol d 1.00E-15 1.00E-16 1.00E-17 - - - "d" ..... u Q) 0 Effluent Concentration Limit= 6E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml Pre 1994 MPC Limit= 4E-12uCi/ml Pre 1994 ALAR A Goal = 1 E-12 uCilml lO ..... .6 Q) LL lO ..... I .... a. <( lO ..... c :::J J lO ..... I C> :::J <( BHV-8 Lead-210 Concentrations (uCi/ml) ------- ' lO ..... I t) 0 lO ..... I (.) Q) 0 <0 ..... .6 Q) LL <0 ..... ~ a. <( - ..... I c: :::J J c, :::J <( ___-A ..... I t) 0 ::::-~ (.) ::J -Cl) c 0 "i -.... c Cl) () c 0 (.) N ('t) ~ E ::J "i: 0 .c I- CO ::> ::1: m ~ (.) :I 1t) ,.... I w '<t 11 - .'!:: E .§ [) ...J :::J C:::lt) o ,.... •-I -w e!o -. C:::T"" B II gm (.)~ "E ct a> a: ..::!< ;:...J W e( C\1 C') '<:!" ..-..-..- I I I w w w 0 0 0 ~ ~ ~ 1\ 9 ~ -onv \ 9~-unr I 9 ~-qa.:J I I ~ s~-oaa -SkPO 1/ s ~ -5nv 1/ s ~-unr v v I \ ~ 1\ v ~-oaa 1.{) (0 ...... CX) Q) ..-..-..-I I Li.J Li.J I w w w 0 0 0 0 0 0 0 ~ ~ ~ '"i areos oo1f ..- ATTACHMENT C BHV AIR SAMPLING LABORATORY RESULTS AND QA/QC EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 888.686.7175 • Helena, MT 877.472.0711 LAB ORA TORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2016 Lab ID: c 16100148-001 Client Sample ID: BHV-1 Analyses Result Units METALS -IN AIR Uranium 1.6E-09 Uranium, Activity 1.1E-15 RADIONUCLIDES -IN AIR Lead 210 1.2E-14 Lead 210 precision(±) 3.7E-15 Lead 210 MDC 3.3E-16 Radium 226 1.8E-16 Radium 226 precision (±) 3.8E-17 Radium 226 MDC 6.8E-18 Thorium 230 8.7E-17 Thorium 230 precision (±) 1.7E-17 Thorium 230 MDC 1.3E-17 Thorium 232 9.5E-18 Thorium 232 precision (±) 1.8E-18 Thorium 232 MDC 1.3E-17 RADIONUCLIDES -IN AIR -PER FILTER Lead 210 1530 Lead 210 precision(±) 457 Lead 210 MDC 40.3 Radium 226 22.1 Radium 226 precision (±) 4.7 Radium 226 MDC 0.84 Thorium 230 10.7 Thorium 230 precision (±) 2.0 Thorium 230 MDC 1.6 Thorium 232 1.2 Thorium 232 precision (±) 0.22 Thorium 232 MDC 1.5 Uranium, Activity 134 CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume 122670500 *** Field data provided by client Report Definitions: RL -Analyte reporting limit. · QCL -Quality control limit. MDC -Minimum detectable concentration mgiL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL pCi/Filter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCi/Filter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter L Report Date: 11/27/16 Collection Date: 09/27/16 Date Received: 10/05/16 Matrix: Filter MCLI Qualifiers RL QCL Method Analysis Date I By 1.5E-10 SW6020 11105116 06:361 smm 1.0E-16 SW6020 11105116 06:361 smm E909.0 1 0125116 23:31 I plj E909.0 10125116 23:311 plj E909.0 1 0125116 23:31 I plj E903.0 11107116 15:371 dmf E903.0 11107116 15:371 dmf E903.0 11107116 15:371 dmf E908.0 10126116 17:131 eng E908.0 10126116 17:131 eng E908.0 10126116 17:131 eng u E908.0 10126116 17:131 eng E908.0 10126116 17:131 eng E908.0 10126116 17:131 eng RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:09 I rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:09/ rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw u RADCALC 11127116 12:231 sec RADCALC 11127/16 12:231 sec RADCALC 11127116 12:231 sec 0.20 RADCALC 1111011613:091 rdw FIELD 09127116 00:00 I *** MCL -Maximum contaminant level. ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 3 of32 EI\ERGY Trust our People. Trust our Data. www.energylab.com Toll Free: 888.235.0515 • 307.235.0515 • F: 307.234.1639 PO Box 247, Casper, WY 82602-0247 • 2393 Salt Creek Hwy (82601) . --I I ...... HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc PROJECT: Jrd Quarter Air 2016 SAMPLEID: BHV-1 REPORT DATE: November 27, 2016 Quarter/Date Sampled Concentration Radionuclide Air Volume ,..ci!mL C16100148-001 natu l.IE-15 Third Quarter 20 16 z3oTh 9E-17 Air Volume in mLs 226Ra 2E-16 1.23E+1 I zwPb . 1.2E-14 23~ 9E-18 +LLD's are from NRC Reg. Guide 4.14 Counting Precision ,..ci!mL N/A 2E-17 4E-17 4E-15 2E-18 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 • L.L.D.+ Eftluent Cone.* % Eftluent MDC11CilmL ,..ci!mL ,..ci!mL Concentration N/A 1E-16 9E-14 1.2E+00 1E-17 1E-16 3E-14 3E-01 7E-18 IE-16 9E-13 2E-02 3E-16 2E-15 6E-13 2.1E+OO 1E-17 N/A 6E-15 2E-01 Page 4 of 32 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LAB ORA TORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Lab ID: C17010161-001 Client Sample ID: BHV-1 Analyses Result Units METALS -IN AIR Uranium 1.4E-09 mgiL Uranium, Activity 9.8E-16 uCilmL RADIONUCLIDES-IN AIR Lead 210 2.2E-14 uCilmL Lead 210 precision(±) 6.7E-15 uCilmL Lead 210 MDC 5.4E-16 uCilmL Radium 226 1 .3E-16 uCilmL Radium 226 precision (±) 2.8E-17 uCilmL Radium 226 MDC 8.4E-18 uCilmL Thorium 230 7.8E-17 uCilmL Thorium 230 precision (±) 1.5E-17 uCilmL Thorium 230 MDC 6.0E-18 uCilmL Thorium 232 4.8E-18 uCilmL Thorium 232 precision (±) 4.1E-18 uCilmL Thorium 232 MDC 6.6E-18 uCilmL RADIONUCLIDES -IN AIR -PER FILTER Lead 210 2780 pCiiFilter Lead 210 precision(±) 831 pCiiFilter Lead 210 MDC 67.7 pCiiFilter Radium 226 15.8 pCiiFilter Radium 226 precision (±) 3.4 pCiiFilter Radium 226 MDC 1.0 pCiiFilter Thorium 230 9.7 pCiiFilter Thorium 230 precision (±) 1.8 pCiiFilter Thorium 230 MDC 0.75 pCiiFilter Thorium 232 0.59 pCiiFilter Thorium 232 precision (±) 0.51 pCiiFilter Thorium 232 MDC 0.82 pCiiFilter Uranium, Activity 122 pCiiFilter RADIOCHEMISTRY AIR FILTER COMPLIANCE Lead 210,% of EFF 3.7E+OO % Lead 210, EFF Day 6.0E-13 uCilmL Lead 210, LLD 2.0E-15 uCilmL Radium 226, % of EFF 1.0E-02 % Radium 226, EFF Week 9.0E-13 uCilmL Radium 226, LLD 1.0E-16 uCilmL Thorium 230, % of EFF 2.6E-01 % Thorium 230, EFF Year 3.0E-14 uCilmL Thorium 230, LLD 1.0E-16 uCilmL Thorium 232, % of EFF 8.0E-02 % Thorium 232, EFF Year 3.0E-14 uCilmL Report RL-Analyte reporting limit. Definitions: QCL -Quality control limit. MDC -Minimum detectable concentration Qualifiers u u MCLI RL QCL 1.5E-10 1 .OE-16 0.20 Report Date: 02/03/17 Collection Date: 12/27/16 DateReceived: 01/06/17 Matrix: Filter Method Analysis Date I By SW6020 01127117 18:521 sf SW6020 01127117 18:521 sf E909.0 01126117 10:151 plj E909.0 01126117 10:151 plj E909.0 01126117 10:151 plj E903.0 01130117 08:20 I dmf E903.0 01130117 08:20 I dmf E903.0 01130117 08:20 I dmf E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec MCL -Maximum contaminant level. ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 3 of 41 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Lab ID: C17010161-001 Client Sample ID: BHV-1 Analyses Result Units RADIOCHEMISTRY AIR FILTER COMPLIANCE Thorium 232, LLD Uranium Natural, % of EFF Uranium Natural, EFF Year Uranium Natural, LLD 1.0E-16 uCi/mL 1.1E+OO % 9.0E-14 uCi/mL 1.0E-16 uCi/mL CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. 124353500 L Qualifiers RL MCU Report Date: 02/03/17 Collection Date: 12/27116 DateReceived: 01/06/17 Matrix: Filter QCL Method Analysis Date I By RADCALC RADCALC RADCALC RADCALC FIELD 02/03/17 15:591 sec 02/03/17 15:591 sec 02/03/17 15:591 sec 02/03/17 15:59 I sec 12/27/16 00:00 I*** MCL-Maximum contaminant level. ND-Not detected at the reporting limit. Page 4 of 41 EI\ERGY ' .... ,' Trust our People. Trust our Data. www.energylab.com I\. ;. P HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 4th Quarter Air 2016 SAMPLE ID: BHV-1 REPORT DATE: February 3, 2017 Quarter/Date Sampled Concentration Radionuclide Air Volume 11CilmL Ci7010161-00I ""u 9.8E-16 Fourth Quarter 2016 23oTh 8E-17 Air Volume in mLs 226Ra IE-16 1.24E+Il 210Pb 2.2E-14 23~h 5E-18 +LLD's are from NRC Reg. Guide 4.14 Counting Precision 11CilmL N/A IE-17 3E-17 7E-15 4E-18 *Effluent Concentration from the NEW I 0 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 MDC 11CilmL N/A 6E-18 8E-18 5E-16 7E-18 Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 : L.L.D.+ Effluent Cone.* o/o Effluent 11CilmL 11CilmL Concentration IE-16 9E-14 l.IE+OO IE-16 3E-14 3E-OI IE-16 9E-13 IE-02 2E-15 6E-13 3.7E+OO N/A 6E-15 8E-02 Page 5 of41 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2016 Lab ID: C16100148-002 Client Sample ID: BHV-2 Analyses Result Units METALS-IN AIR Uranium 6.2E-10 Uranium, Activity 4.2E-16 RADIONUCLIDES -IN AIR Lead 210 1.0E-14 Lead 210 precision (±) 3.1 E-15 Lead 210 MDC 1.9E-16 Radium 226 8.1E-17 Radium 226 precision (±) 1.9E-17 Radium 226 MDC 6.3E-18 Thorium 230 6.9E-17 Thorium 230 precision (±) 1.3E-17 Thorium 230 MDC 5 .. 2E-17 Thorium 232 -9.4E-18 Thorium 232 precision (±) 2.2E-17 Thorium 232 MDC 5.2E-17 RADIONUCLIDES -IN AIR -PER FILTER Lead 210 1280 Lead 210 precision (±) 376 Lead 210 MDC 23.0 Radium 226 9.9 Radium 226 precision (±) 2.3 Radium 226 MDC 0.78 Thorium 230 8.5 Thorium 230 precision (±) 1.6 Thorium 230 MDC 6.4 Thorium 232 -1 .1 Thorium 232 precision (±) 2.6 Thorium 232 MDC 6.4 Uranium, Activity 51 .6 CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume 122413300 ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. MDC -Minimum detectable concentration mg/L uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL pCi!Filter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter L Qualifiers u u RL 1.5E-10 1.0E-16 0.20 Report Date: 11/27/16 Collection Date: 09/27/16 DateReceived: 10/05116 Matrix: Filter ------ MCLI QCL Method Analysis Date I By SW6020 11105116 06:42 I smm SW6020 11105116 06:42 I smm E909.0 10125116 23:34 I eli-cs E909.0 10125116 23:34 I eli-cs E909.0 10125116 23:341 eli-cs E903.0 11107116 15:37 I dmf E903.0 11107116 15:37 I dmf E903.0 11107116 15:37 I dmf E908.0 10126116 17:131 eng E908.0 10126116 17:131 eng E908.0 10126116 17:13 I eng E908.0 10126116 17:131 eng E908.0 10/26116 17:131 eng E908.0 10126116 17:131 eng RADCALC 11127116 11 :05 I sec RADCALC 11127116 11 :05 I sec RADCALC 11/2711611:051sec RADCALC 11127116 11 :051 sec RADCALC 11127116 11 :051 sec RADCALC 11127116 11 :051 sec RADCALC 11127116 11 :05 I sec RADCALC 11127116 11 :05 I sec RADCALC 11127116 11 :051 sec RADCALC 11127116 12:23 I sec RADCALC 11127116 12:231 sec RADCALC 11127116 12:23 I sec RADCALC 11127116 11 :051 sec FIELD 09127116 00:00 I*** MCL -Maximum contaminant level. ND-Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 5 of 32 EI\ERGY ,, ''• ' I • --.. Trust our People. Trust our Data. www.energylab.com Toll Free: 888.235.0515 o 307.235.0515 oF: 307.234.1639 PO Box 247, Casper, WY 82602-0247 o 2393 Salt Creek Hwy (82601) ,, --HIGH VOLUME AIR SAMPLING REPORT . ·, ... . ·. CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 3rd Quarter Air 2016 SAMPLE ID: BHV-2 • • REPORT DATE: November 27, 2016 Quarter/Date Sampled Concentration Radionuclide Air Volume ,..cvmL c 16100148-002 ""'U 4E-16 Third Quarter 2016 23fJTh 7E-17 Air Volume in mLs 226Ra 8E-17 1.22E+II 210Pb l.OE-14 212Th -9E-18 +LLD's are from NRC Reg. Guide 4.14 Counting Precision ,..cvmL N/A IE-17 2E-17 3E-15 2E-17 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 .. L.L.D.+ Effluent Cone.* %Effluent MDCJ!CilmL ,..cilmL ,..cvmL Concentration N/A IE-16 9E-14 5E-01 5E-17 IE-16 3E-14 2E-01 6E-18 IE-16 9E-13 9E-03 2E-16 2E-15 6E-13 1.7E+OO 5E-17 N/A 6E-15 -2E-OI Page 6 of32 EI\ERGY Trust our People. Trust our Data. www.e n e rgyla b. com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Lab ID: C17010161-002 Client Sample ID: BHV-2 Analyses Result Units METALS -IN AIR Uranium 6.1E-10 mgiL Uranium, Activity 4.1E-16 uCilmL RADIONUCLIDES -IN AIR Lead 210 2.1E-14 uCilmL Lead 210 precision (±) 6.2E-15 uCilmL Lead 210 MDC 5.3E-16 uCilmL Radium 226 5.0E-17 uCilmL Radium 226 precision (±) 1.3E-17 uCilmL Radium 226 MDC 8.2E-18 uCilmL Thorium 230 1.9E-17 uCilmL Thorium 230 precision (±) 3.7E-18 uCilmL Thorium 230 MDC 3.3E-18 uCilmL Thorium 232 2.2E-18 uCilmL Thorium 232 precision (±) 1.8E-18 uCilmL Thorium 232 MDC 2.9E-18 uCilmL RADIONUCLIDES -IN AIR -PER FILTER Lead 210 2590 pCiiFilter Lead 21 0 precision (±) 776 pCiiFilter Lead 210 MDC 66.6 pCiiFilter Radium 226 6.2 pCiiFilter Radium 226 precision (±) 1.7 pCiiFilter Radium 226 MDC 1.0 pCiiFilter Thorium 230 2.4 pCiiFilter Thorium 230 precision (±) 0.46 pCiiFilter Thorium 230 MDC 0.42 pCiiFilter Thorium 232 0.27 pCiiFilter Thorium 232 precision (±) 0.23 pCi!Filter Thorium 232 MDC 0.36 pCiiFilter Uranium, Activity 51.5 pCi!Filter RADIOCHEMISTRY AIR FILTER COMPLIANCE Lead 210,% of EFF 3.5E+OO % Lead 210, EFF Day 6.0E-13 uCilmL Lead 210, LLD 2.0E-15 uCilmL Radium 226, % of EFF 6.0E-03 % Radium 226, EFF Week 9.0E-13 uCilmL Radium 226, LLD 1.0E-16 uCilmL Thorium 230, % of EFF 6.0E-02 % Thorium 230, EFF Year 3.0E-14 uCilmL Thorium 230, LLD 1.0E-16 uCilmL Thorium 232, % of EFF 4.0E-02 % Thorium 232, EFF Year 3.0E-14 uCilmL Report RL-Analyte reporting limit. Definitions: QCL-Quality control limit. MDC -Minimum detectable concentration Qualifiers u u MCL/ RL QCL 1.5E-10 1.0E-16 0.20 Report Date: 02/03/17 Collection Date: 12/27/16 DateReceived: 01/06/17 Matrix: Filter Method Analysis Date I By SW6020 01117117 17:471 sf SW6020 01117117 17:471 sf E909.0 01126117 10:231 plj E909.0 01126117 10:231 plj E909.0 01126117 10:231 plj E903.0 01130117 08:20 I dmf E903.0 01130117 08:20 I dmf E903.0 01130117 08:20 I dmf E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng E908.0 01124117 09:24 I eng E908.0 01124117 09:241 eng E908.0 01124117 09:24 I eng RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:591 sec MCL-Maximum contaminant level. ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 6 of 41 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.888.7175 • Helena, MT 877.472.0711 LAB ORA TORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Lab ID: C17010161-002 Client Sample ID: BHV-2 Analyses Result Units RADIOCHEMISTRY AIR FILTER COMPLIANCE Thorium 232, LLD 1.0E-16 Uranium Natural, % of EFF 4.6E-01 Uranium Natural, EFF Year 9.0E-14 Uranium Natural, LLD 1.0E-16 CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume *** Field data provided by client Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. 125156400 uCi/mL % uCi/mL uCilmL L Qualifiers RL MCLI Report Date: 02/03/17 Collection Date: 12/27116 DateReceived: 01/06/17 Matrix: Filter QCL Method Analysis Date I By RADCALC 02/03117 15:59 I sec RADCALC 02/03/1715:59/ sec RADCALC 02/03/17 15:59 I sec RADCALC 02103117 15:59 I sec FIELD 12/27116 00:00 I*** MCL-Maximum contaminant level. NO -Not detected at the reporting limit. Page 7 of 41 EI\ERGY ', \ '• I I Trust our People. Trust our Data. www.energylab.com HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 4th Quarter Air 2016 SAMPLE ID: BHV-2 REPORT DATE: February 3, 2017 Quarter/Date Sampled Concentration Radio nuclide Air Volume pCilmL C17010161-002 ""'U 4E-16 Fourth Quarter 20 16 23oTh 2E-17 Air Volume in mLs 226Ra 5E-17 1.25E+ll 21oPb 2.1E-14 232Th 2E-18 +LLD's are from NRC Reg. Guide 4.14 Counting Precision pCi/mL N/A 4E-18 IE-17 6E-15 2E-18 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 MDCpCilmL N/A 3E-18 8E-18 5E-16 3E-18 Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 -I L.L.D.+ Effiuent Cone.* % Emuent pCilmL pCilmL Concentration 1E-16 9E-14 5E-01 IE-16 3E-14 6E-02 IE-16 9E-13 6E-03 2E-15 6E-13 3.5E+OO N/A 6E-15 4E-02 Page 8 of41 EI\ERGY •' Trust our People. Trust our Data. www.energylab.corn Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Statioo, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0111 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2016 Lab ID: c 16100148-003 Client Sample ID: BHV-4 Analyses Result Units METALS -IN AIR Uranium 9.2E-09 Uranium, Activity 6.2E-15 RADIONUCLIDES -IN AIR Lead 210 3.4E-16 Lead 210 precision (±) 1.2E-16 Lead 210 MDC 8.7E-17 Radium 226 2.2E-15 Radium 226 precision (±) 4.1E-16 Radium 226 MDC 6.5E-18 Thorium 230 4.4E-16 Thorium 230 precision (±) 8.4E-17 Thorium 230 MDC 1.1E-17 Thorium 232 7.1E-18 Thorium 232 precision (±) 6.0E-18 Thorium 232 MDC 9.3E-18 RADIONUCLIDES -IN AIR -PER FILTER Lead 210 42.0 Lead 210 precision(±) 14.3 Lead 210 MDC 10.7 Radium 226 267 Radium 226 precision (±) 50.6 Radium 226 MDC 0.79 Thorium 230 53.8 Thorium 230 precision (±) 10.2 Thorium 230 MDC 1.3 Thorium 232 0.87 Thorium 232 precision (±) 0.74 Thorium 232 MDC 1.1 Uranium, Activity 763 CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume 122222200 ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. MDC -Minimum detectable concentration mgll uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCi/Filter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter L Report Date: 11/27116 Collection Date: 09/27/16 Date Received: 10/05/16 Matrix: Filter MCU Qualifiers RL QCL Method Analysis Date I By 1.5E-10 SW6020 11/05116 06:48 I smm 1.0E-16 SW6020 11105116 06:48 I smm E909.0 10126116 02:47 I plj E909.0 10126116 02:47 I plj E909.0 10126116 02 :47 I plj E903.0 11107116 15:37 I dmf E903.0 11107116 15:37 I dmf E903.0 11107116 15:371 dmf E908.0 10126116 17:131 eng E908.0 10126116 17:131 eng E908.0 1012611617:13 I eng u E908.0 10126116 17:13 I eng E908.0 10126116 17:13 I eng E908.0 10126116 17:13 I eng RADCALC 11110116 13:09 I rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:09 I rdw RADCALC 1111011613:091 rdw RADCALC 1111011613:09 I rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:09 I rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw u RADCALC 1112711612:231 sec RADCALC 11127116 12:231 sec RADCALC 11127116 12:23 I sec 0.20 RADCALC 11110116 13:09 I rdw FIELD 09127116 00:00 I ••• MCL-Maximum contaminant level. ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 7 of32 Er\ERGY . ' ' Trust our People. Trust our Data. www.energylab.com Toll Free: 888.235.0515 • 307.235.0515 • F: 307.234.1639 PO Box 247, Casper, WY 82602-0247 • 2393 Salt Creek Hwy (82601) HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 3rd Quarter Air 2016 SAMPLE ID: BHV -4 REPORT DATE: November 27,2016 Quarter/Date Sampled Concentration Radionuclide Air Volume J.!CilmL C16100148-003 nalu 6.2E-15 Third Quarter 2016 230Th 4E-16 Air Volume in mLs 226Ra 2.2E-15 l.22E+ll 210Pb 3E-16 232Th 7E-18 +LLD's are from NRC Reg. Guide 4.14 Counting Precision J.!CilmL N/A 8E-l7 4E-16 IE-16 6E-18 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 L.L.D.+ Effluent Cone.* %Effluent MDCJ.!CilmL J.tCilmL J.!Ci/mL Concentration N/A 1E-16 9E-14 6.9E+00 1E-l7 1E-16 3E-14 IE+OO 6E-18 IE-16 9E-13 2.4E-01 9E-17 2E-15 6E-13 6E-02 9E-18 N/A 6E-15 IE-01 Page 8 of32 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Lab ID: C1701 0161-003 Client Sample ID: BHV-4 Analyses Result Units METALS -IN AIR Uranium 6.1 E-09 mgiL Uranium, Activity 4.1 E-15 uCilmL RADIONUCLIDES -IN AIR Lead 210 2.2E-14 uCilmL Lead 210 precision (±) 6.5E-15 uCilmL Lead 210 MDC 5.5E-16 uCilmL Radium 226 4.8E-16 uCilmL Radium 226 precision (±) 9.4E-17 uCilmL Radium 226 MDC 8.4E-18 uCilmL Thorium 230 3.0E-16 uCilmL Thorium 230 precision (±) 5.6E-17 uCilmL Thorium 230 MDC 9.8E-18 uCilmL Thorium 232 4.5E-18 uCilmL Thorium 232 precision (±) 4.1E-18 uCilmL Thorium 232 MDC 6.6E-18 uCilmL RADIONUCLIDES -IN AIR -PER FILTER Lead 210 2700 pCiiFilter Lead 210 precision (±) 807 pCiiFilter Lead 210 MDC 69.1 pCiiFilter Radium 226 59.8 pCiiFilter Radium 226 precision (±) 11.7 pCi!Filter Radium 226 MDC 1.0 pCiiFilter Thorium 230 37.0 pCiiFilter Thorium 230 precision (±) 7.0 pCiiFilter Thorium 230 MDC 1.2 pCiiFilter Thorium 232 0.57 pCiiFilter Thorium 232 precision (±) 0.51 pCiiFilter Thorium 232 MDC 0.83 pCiiFilter Uranium, Activity 512 pCiiFilter RADIOCHEMISTRY AIR FILTER COMPLIANCE Lead 210,% of EFF 3.6E+OO % Lead 210, EFF Day 6.0E-13 uCilmL Lead 210, LLD 2.0E-15 uCilmL Radium 226, % of EFF 5.0E-02 % Radium 226, EFF Week 9.0E-13 uCilmL Radium 226, LLD 1 .OE-16 uCilmL Thorium 230, % of EFF 9.9E-01 % Thorium 230, EFF Year 3.0E-14 uCilmL Thorium 230, LLD 1.0E-16 uCilmL Thorium 232, % of EFF 8.0E-02 % Thorium 232, EFF Year 3.0E-14 uCilmL Report RL -Analyte reporting limit. Definitions: QCL-Quality control limit. MDC -Minimum detectable concentration Qualifiers u u MCLI RL QCL 1 .5E-1 0 1 .OE-16 0.20 Report Date: 02/03/17 Collection Date: 12/27/16 DateReceived: 01/06/17 Matrix: Filter Method Analysis Date I By SW6020 01127117 19:12 I sf SW6020 01127117 19:12 I sf E909.0 01126117 10:33 I plj E909.0 01126117 10:33 I plj E909.0 01126117 10:331 plj E903.0 01130117 08:20 I dmf E903.0 01130117 08:20 I dmf E903.0 01130117 08:20 I dmf E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng E908.0 01124117 09:24 I eng E908.0 01124117 09:24 I eng E908.0 01124117 09:24 I eng RADCALC 02103117 15:57 I sec RADCALC 02103117 15:571 sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec MCL-Maximum contaminant level. ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 9 of 41 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Collage Station, TX 888.890.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 LabiD: C17010161-003 Client Sample ID: BHV-4 Analyses Result Units RADIOCHEMISTRY AIR FILTER COMPLIANCE Thorium 232, LLD 1.0E-16 Uranium Natural, % of EFF 4.6E+OO Uranium Natural, EFF Year 9.0E-14 Uranium Natural, LLD 1.0E-16 CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume *** Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. 124798300 uCi/mL % uCilmL uCilmL L Qualifiers RL MCU Report Date: 02/03/17 Collection Date: 12/27/16 DateReceived: 01/06/17 Matrix: Filter QCL Method Analysis Date I By RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02/03117 15:59 I sec FIELD 12/27/16 00:00 , ••• MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 41 EN:RGY . ·' , = Trust our People. Trust our Data. www.energylab.com HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 4th Quarter Air 2016 SAMPLE ID: BHV-4 REPORT DATE: February 3, 2017 Quarter/Date Sampled Concentration Radionucllde Air Volume J!CilmL Cl7010161-003 natu 4.1E-15 Fourth Quarter 20 16 2JoTh 3E-16 Air Volume in mLs 226Ra 5E-16 1.25E+ll 21oPb 2.2E-14 23~h 5E-18 +LLD's are from NRC Reg. Guide 4.14 Counting Precision !lCilmL N/A 6E-17 9E-17 6E-15 4E-18 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 MDC J!CilmL N/A 1E-17 8E-18 6E-16 7E-18 Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 L.L.D.+ Effluent Cone.* %Effluent J!CilmL JlCi/mL Concentration 1E-16 9E-14 4.6E+00 IE-16 3E-14 IE+OO 1E-16 9E-13 5E-02 2E-15 6E-13 3.6E+OO N/A 6E-15 8E-02 Page 11 of 41 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 o Casper, WY 888.235.0515 College Station, TX 888.690.2218 o Gillette, WY 866.686.7175 o Helena, MT 877.472.0711 LAB ORA TORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2016 Lab ID: C16100148-004 Client Sample ID: BHV-5 Analyses Result Units METALS -IN AIR Uranium 1.0E-08 Uranium, Activity 7.1E-15 RADIONUCLIDES -IN AIR Lead 210 2.9E-16 Lead 210 precision(±) 1.0E-16 Lead 210 MDC 8.5E-17 Radium 226 1.1E-15 Radium 226 precision (±) 2.2E-16 Radium 226 MDC 6.4E-18 Thorium 230 7.6E-16 Thorium 230 precision (±) 1.4E-16 Thorium 230 MDC 1.8E-17 Thorium 232 3.0E-17 Thorium 232 precision (±) 5.7E-18 Thorium 232 MDC 1.9E-17 RADIONUCLIDES -IN AIR -PER FILTER Lead 210 36.0 Lead 210 precision(±) 12.6 Lead 210 MDC 10.4 Radium 226 139 Radium 226 precision (±) 26.5 Radium 226 MDC 0.79 Thorium 230 92.9 Thorium 230 precision (±) 17.6 Thorium 230 MDC 2.2 Thorium 232 3.6 Thorium 232 precision (±) 0.69 Thorium 232 MDC 2.4 Uranium, Activity 863 CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume 122343700 ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. MDC -Minimum detectable concentration mgiL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL pCiiFilter pCiiFilter pCiiFilter pCi!Filter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCi/Filter pCiiFilter L Qualifiers MCLI RL QCL 1.5E-10 1.0E-16 0.20 Report Date: 11/27/16 Collection Date: 09/27/16 DateReceived: 10/05/16 Matrix: Filter Method Analysis Date I By SW6020 11105116 07:20 I smm SW6020 11105116 07:20 I smm E909.0 10126116 04:48 I plj E909.0 10126116 04:48 I plj E909.0 10126116 04:48 I plj E903.0 11107116 15:37 I dmf E903.0 11107116 15:37 I dmf E903.0 11107116 15:371 dmf E908.0 10126116 17:131 eng E908.0 10126116 17:131 eng E908.0 10126116 17:131 eng E908.0 10126116 17:131 eng E908.0 10126116 17:13 I eng E908.0 1012611617:131 eng RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 1111 0116 13:09 I rdw RADCALC 11127116 12:231 sec RADCALC 11127116 12:231 sec RADCALC 11127116 12:231 sec RADCALC 11110116 13:091 rdw FIELD 09127116 00:00 I*** MCL-Maximum contaminant level. ND -Not detected at the reporting limit. Page 9 of32 EI\ERGY ' ' o/ I Trust our People. Trust our Data. www.energylab.rom Toll Free: 888.235.0515 • 307.235.0515 • F: 307.234.1639 PO Box 247, Casper, WY 82602-0247 • 2393 Salt Creek Hwy (82601) HIGH VOLUME AIR SAMPLING REPORT . .. CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 3rd Quarter Air 2016 SAMPLE ID: BHV -5 REPORT DATE: November 27,2016 Quarter/Date Sampled Concentration Air Volume Radionuclide ~Ci/rnL Cl6100148-004 natu 7.1E-15 Third Quarter 2016 23oTh 8E-16 Air Volume in mLs 226Ra I.IE-15 1.22E+11 210Pb 3E-16 232Th 3E-17 +LLD's are from NRC Reg. Guide 4.14 Counting Precision ~CilmL N/A 1E-16 2E-16 JE-16 6E-18 *Effluent Concentration from the NEW I 0 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 .... ~· L.L.D.+ Effluent Cone.* %Effluent MDC ~CilmL ~Ci/mL ~Ci/mL Concentration N/A lE-16 9E-14 7.8E+00 2E-17 IE-16 3E-14 3E+00 6E-18 IE-16 9E-13 1.3E-Ol 8E-17 2E-15 6E-13 5E-02 2E-17 N/A 6E-15 5E-OI Page 10 of 32 EI\ERGY Trust our People. Trust our Data. www.energylab.(om Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 817.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Lab ID: C17010161-004 Client Sample ID: BHV-5 Analyses Result Units METALS -IN AIR Uranium 7.5E-09 mg/L Uranium, Activity 5.1E-15 uCilmL RADIONUCLIDES -IN AIR Lead 210 2.1E-14 uCilmL Lead 210 precision(±) 6.2E-15 uCilmL Lead 210 MDC 5.3E-16 uCilmL Radium 226 9.6E-16 uCilmL Radium 226 precision (±) 1.8E-16 uCilmL Radium 226 MDC 8.4E-18 uCilmL Thorium 230 6.6E-16 uCilmL Thorium 230 precision (±) 1.2E-16 uCilmL Thorium 230 MDC 1.0E-17 uCilmL Thorium 232 1.3E-17 uCilmL Thorium 232 precision (±) 2.5E-18 uCilmL Thorium 232 MDC 1.0E-17 uCilmL RADIONUCLIDES -IN AIR -PER FILTER Lead 210 2600 pCiiFilter Lead 210 precision(±) 777 pCiiFilter Lead 210 MDC 66.7 pCiiFilter Radium 226 120 pCiiFilter Radium 226 precision (±) 23.0 pCi/Filter Radium 226 MDC 1.1 pCiiFilter Thorium 230 82.4 pCiiFilter Thorium 230 precision (±) 15.6 pCi!Filter Thorium 230 MDC 1.3 pCiiFilter Thorium 232 1.7 pCi!Filter Thorium 232 precision (±) 0.32 pCiiFilter Thorium 232 MDC 1.3 pCi/Filter Uranium, Activity 635 pCi/Filter RADIOCHEMISTRY AIR FILTER COMPLIANCE Lead 210, % of EFF 3.4E+OO % Lead 210, EFF Day 6.0E-13 uCilmL Lead 210, LLD 2.0E-15 uCilmL Radium 226, % of EFF 1.1 E-01 % Radium 226, EFF Week 9.0E-13 uCilmL Radium 226, LLD 1.0E-16 uCilmL Thorium 230, % of EFF 2.2E+OO % Thorium 230, EFF Year 3.0E-14 uCilmL Thorium 230, LLD 1.0E-16 uCilmL Thorium 232, % of EFF 2.2E-01 % Thorium 232, EFF Year 3.0E-14 uCilmL Report RL -Analyte reporting limit. Definitions: QCL -Quality control limit. MDC -Minimum detectable concentration Qualifiers MCL/ RL QCL 1.5E-10 1.0E-16 0.20 Report Date: 02/03/17 Collection Date: 12/27/16 Date Received: 01/06/17 Matrix: Filter Method Analysis Date I By SW6020 01127117 19:141 sf SW6020 01127117 19:141 sf E909.0 01126117 1 0:42 I plj E909.0 01126117 10:421 plj E909.0 01126117 1 0:42 I plj E903.0 01130117 08:20 I dmf E903.0 01130117 08:20 I dmf E903.0 01130117 08:20 I dmf E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng E908.0 01124117 09:241 eng RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec .RADCALC 02103117 15:571 sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:591 sec MCL-Maximum contaminant level. NO -Not detected at the reporting limit. Page 12 of 41 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Lab ID: C17010161-004 Client Sample ID: BHV-5 Analyses Result Units RADIOCHEMISTRY AIR FILTER COMPLIANCE Thorium 232, LLD 1.0E-16 Uranium Natural, % of EFF 5.6E+OO Uranium Natural, EFF Year 9.0E-14 Uranium Natural, LLD 1.0E-16 CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. 125655300 uCi/mL % uCilmL uCilmL L Qualifiers RL MCU Report Date: 02/03/17 Collection Date: 12/27116 DateReceived: 01/06/17 Matrix: Filter QCL Method Analysis Date I By RADCALC 02/03/17 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103/17 15:59 I sec FIELD 12127116 00:00 I ••• MCL-Maximum contaminant level. ND -Not detected at the reporting limit. Page 13 of41 EI\ERGY •' •I '"I, H • I Trust our People. Trust our Data. www.energylab.com HIGH VOLUME AIR SAMPLING REPORT '. ' CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 4th Quarter Air 2016 SAMPLE ID: BHV-5 REPORT DATE: February 3, 2017 Quarter/Date Sampled Concentration Radionuclide Air Volume J1CilmL C 170 I 0161-004 natu S.IE-15 Fourth Quarter 20 16 23~ 7E-16 Air Volume in mLs 226Ra 9.6E-16 1.26E+ll 21oPb 2.1E-14 232Th IE-17 +LLD's are from NRC Reg. Guide 4.14 Counting Precision J1CilmL N/A IE-16 2E-16 6E-15 3E-18 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 MDC JICi/mL N/A IE-17 8E-18 5E-16 IE-17 Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Gillette, WY 866.686.7175 • Helena, MT 877.412.0711 L.L.D.+ Effluent Cone.* % Emuent J1CilmL J1Ci/mL Concentration IE-16 9E-14 5.6E+00 IE-16 3E-14 2E+00 IE-16 9E-13 I.IE-01 2E-15 6E-13 3.4E+00 N/A 6E-15 2E-OI Page 14 of 41 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2016 Lab ID: C161 00148-005 Client Sample ID: BHV-6 Analyses Result Units METALS -IN AIR Uranium 1.0E-08 Uranium, Activity 6.9E-15 RADIONUCLIDES -IN AIR Lead 210 3.2E-15 Lead 210 precision(±) 9.5E-16 Lead 210 MDC 1.7E-16 Radium 226 7.2E-16 Radium 226 precision (±) 1.4E-16 Radium 226 MDC 6.3E-18 Thorium 230 4.0E-16 Thorium 230 precision (±) 7.6E-17 Thorium 230 MDC 2.6E-17 Thorium 232 1.2E-17 Thorium 232 precision (±) 2.4E-18 Thorium 232 MDC 1.9E-17 RADIONUCLIDES -IN AIR-PERFIL TER Lead 210 386 Lead 210 precision (±) 116 Lead 210 MDC 21.3 Radium 226 88.5 Radium 226 precision (±) 17.1 Radium 226 MDC 0.77 Thorium 230 48.9 Thorium 230 precision (±) 9.3 Thorium 230 MDC 3.2 Thorium 232 1.5 Thorium 232 precision (±) 0.29 Thorium 232 MDC 2.3 Uranium, Activity 846 CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume 122275800 *** Field data provided by client Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. MDC -Minimum detectable concentration mgiL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCi/Filter pCiiFilter pCi/Filter L Report Date: 11/27116 Collection Date: 09/27/16 Date Received: 10/05/16 Matrix: Filter MCL/ Qualifiers RL QCL Method Analysis Date I By 1.5E-10 SW6020 11105116 07:26 I smm 1.0E-16 SW6020 11105116 07:261 smm E909.0 10126116 06:551 plj E909.0 10126116 06:55 I plj E909.0 10126116 06:55 I plj E903.0 11107116 15:37 I dmf E903.0 11107116 15:37 I dmf E903.0 11107116 15:37 I dmf E908.0 10126116 17:13 I eng E908.0 1012611617:13 I eng E908.0 10126116 17:13 I eng u E908.0 10126116 17:13 I eng E908.0 10126116 17:13 I eng E908.0 10126116 17:13 I eng RADCALC 11110116 13:09 I rdw RADCALC 11110116 13:09 I rdw RADCALC 11110116 13:09 I rdw RADCALC 1111011613:09 I rdw RADCALC 1111011613:09 I rdw RADCALC 11110116 13:09 I rdw RADCALC 1111011613:09 I rdw RADCALC 1111011613:09 I rdw RADCALC 11110116 13:09 I rdw u RADCALC 11127116 12:23 I sec RADCALC 11127116 12:23 I sec RADCALC 1112711612:231sec 0.20 RADCALC 1111011613:091 rdw FIELD 09127116 00:00 I*** MCL-Maximum contaminant level. ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 11 of 32 E~RGY ' ',· I'• Trust our People. Trust our Data. www.energylab.com Toll Free: 888.235.0515 • 307.235.0515 • F: 307.234.1639 PO Box 247, Casper, WY 82602-0247 • 2393 Salt Creek Hwy (82601) HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 3rd Quarter Air 2016 SAMPLE ID: BHV-6 I ' REPORT DATE: November 27,2016 Quarter/Date Sampled Concentration Radio nuclide Air Volume J.1CilmL c 16100148-005 nalu 6.9E-15 Third Quarter 2016 23oTh 4E-16 Air Volume in mLs 226Ra 7E-16 1.22E+11 210Pb 3E-15 232Th 1E-17 +LLD's are from NRC Reg. Guide 4.14 Counting Precision JJCilmL N/A SE-17 1E-16 1E-15 2E-18 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 L.L.D.+ Effiuent Cone.* % Effiuent MDCJ.1CilmL J.1CilmL J.1Ci/mL Concentration N/A 1E-16 9E-14 7.7E+00 3E-17 1E-16 3E-14 1E+OO 6E-18 IE-16 9E-13 SE-02 2E-16 2E-15 6E-13 SE-01 2E-17 N/A 6E-15 2E-OI Page 12 of 32 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LAB ORA TORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 02/03/17 Project: 4th Quarter Air 2016 Collection Date: 12/27116 Lab ID: C17010161-005 DateReceived: 01/06/17 Client Sample ID: BHV-6 Matrix: Filter MCU Analyses Result Units Qualifiers RL QCL Method Analysis Date I By METALS -IN AIR Uranium 1.3E-08 mgiL 1.5E-1 0 SW6020 01127117 19:171 sf Uranium, Activity 8.9E-15 uCilmL 1.0E-16 SW6020 01127117 19:171 sf RADIONUCLIDES -IN AIR Lead 210 2.1 E-14 uCilmL E909.0 01126117 10:51 I plj Lead 210 precision(±) 6.4E-15 uCilmL E909.0 01126117 10:51 I plj Lead 210 MDC 5.4E-16 uCilmL E909.0 01126117 10:51 I plj Radium 226 4.8E-16 uCilmL E903.0 01130117 08:20 I dmf Radium 226 precision (±) 9.4E-17 uCilmL E903.0 01130117 08:20 I dmf Radium 226 MDC 8.8E-18 uCilmL E903.0 01130117 08:20 I dmf Thorium 230 3.3E-16 uCilmL E908.0 01124117 09:251 eng Thorium 230 precision (±) 6.4E-17 uCilmL E908.0 01124117 09:25 I eng Thorium 230 MDC 1.2E-17 uCilmL E908.0 01124117 09:25 I eng Thorium 232 9.5E-18 uCilmL u E908.0 01124117 09:251 eng Thorium 232 precision (±) 1.8E-18 uCilmL E908.0 01124117 09:251 eng Thorium 232 MDC 1.2E-17 uCilmL E908.0 01124117 09:25 I eng RADIONUCLIDES -IN AIR -PER Fll TER Lead 210 2680 pCiiFilter RADCALC 02103117 15:571 sec Lead 210 precision (±) 800 pCiiFilter RADCALC 02103117 15:57 I sec Lead 210 MDC 67.1 pCiiFilter RADCALC 02103117 15:57 I sec Radium 226 60.1 pCiiFilter RADCALC 02103117 15:57 I sec Radium 226 precision (±) 11.8 pCiiFilter RADCALC 02103117 15:57 I sec Radium 226 MDC 1.1 pCiiFilter RADCALC 02103117 15:57 I sec Thorium 230 41 .9 pCiiFilter RADCALC 02103117 15:57 I sec Thorium 230 precision (±) 8.0 pCiiFilter RADCALC 02103117 15:57 I sec Thorium 230 MDC 1.5 pCiiFilter RADCALC 02103117 15:57 I sec Thorium 232 1.2 pCi!Filter u RADCALC 02103117 15:57 I sec Thorium 232 precision (±) 0.23 pCiiFilter RADCALC 02103117 15:57 I sec Thorium 232 MDC 1.5 pCiiFilter RADCALC 0210311715:571sec Uranium, Activity 1110 pCiiFilter 0.20 RADCALC 02103117 15:57 I sec RADIOCHEMISTRY AIR FILTER COMPLIANCE Lead 210,% of EFF 3.6E+OO % RADCALC 02103117 15:59 I sec Lead 210, EFF Day 6.0E-13 uCilmL RADCALC 02103117 15:591 sec Lead 210, LLD 2.0E-15 uCilmL RADCALC 02103117 15:59 I sec Radium 226, % of EFF 5.0E-02 % RADCALC 02103117 15:591 sec Radium 226, EFF Week 9.0E-13 uCilmL RADCALC 02103117 15:59 I sec Radium 226, LLD 1.0E-16 uCilmL RADCALC 02103117 15:59 I sec Thorium 230, % of EFF 1.1E+OO % RADCALC 02103117 15:59 I sec Thorium 230, EFF Year 3.0E-14 uCilmL RADCALC 02103117 15:59 I sec Thorium 230, LLD 1.0E-16 uCilmL RADCALC 02103117 15:59 I sec Thorium 232, % of EFF 1.6E-01 % RADCALC 02103117 15:59 I sec Thorium 232, EFF Year 3.0E-14 uCilmL RADCALC 02103117 15:591 sec Report RL-Analyte reporting limit. MCL-Maximum contaminant level. Definitions: QCL-Quality control limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration Page 15 of 41 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.412.0111 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: lab ID: Client Sample ID: Energy Fuels Resources (USA) Inc 4th Quarter Air 2016 C17010161-005 BHV-6 Report Date: 02/03/17 Collection Date: 12/27116 DateReceived: 01/06/17 Matrix: Filter -------~----------- Analyses Result Units RADIOCHEMISTRY AIR Fll TER COMPLIANCE Thorium 232, LLD 1.0E-16 Uranium Natural, % of EFF 9.8E+OO Uranium Natural, EFF Year 9.0E-14 Uranium Natural, LLD 1.0E-16 CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume *** Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. 125092600 uCilmL % uCilmL uCilmL L MCL/ Qualifiers RL QCL Method Analysis Date I By RADCALC 02103117 15:59 I sec RADCALC 02103/17 15:59 I sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:59 I sec FIELD 12127116 00:00 I*** MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 16 of41 EI\ERGY '' . ,, ',.' / Trust our People. Trust our Data. www.energylab.com HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 4th Quarter Air 2016 SAMPLE ID: BHV -6 REPORT DATE: February 3, 2017 Quarter/Date Sampled Concentration Radio nuclide Air Volume pCilmL Cl7010161-005 na•u 8.9E-15 Fourth Quarter 2016 230Th 3E-16 Air Volume in mLs 226Ra 5E-16 1.25E+l1 210Pb 2.1E-14 232Th 1E-17 +LLD's are from NRC Reg. Guide 4.14 Counting Precision pCilmL N/A 6E-17 9E-17 6E-15 2E-18 *Effluent Concentration from the NEW I 0 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 MDCpCilmL N/A lE-17 9E-18 5E-16 1E-17 Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 L.L.D.+ Effluent Cone.* %Effluent pCilmL pCi/mL Concentration lE-16 9E-14 9.8E+00 1E-16 3E-14 1E+00 lE-16 9E-13 5E-02 2E-15 6E-13 3.6E+00 N/A 6E-15 2E-01 Page 17 of 41 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LAB ORA TORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Energy Fuels Resources (USA) Inc 3rd Quarter Air 2016 C16100148-006 Report Date: 11/27/16 Collection Date: 09/27/16 DateReceived: 10/05/16 Client Sample ID: BHV-7 Matrix: Filter Analyses Result Units METALS -IN AIR Uranium 3.8E-09 Uranium, Activity 2.6E-15 RADIONUCLIDES -IN AIR Lead 210 2.8E-15 Lead 210 precision(±) 8.5E-16 Lead 210 MDC 1.6E-16 Radium 226 4.1 E-16 Radium 226 precision (±) 8.0E-17 Radium 226 MDC 5.9E-18 Thorium 230 1.7E-16 Thorium 230 precision (±) 3.3E-17 Thorium 230 MDC 2.8E-18 Thorium 232 5.5E-18 Thorium 232 precision (±) 2.4E-18 Thorium 232 MDC 2.6E-18 RADIO NUCLIDES -IN AIR -PER Fll TER Lead 210 347 Lead 210 precision (±) 105 Lead 210 MDC 20.0 Radium 226 50.0 Radium 226 precision (±) 9.8 Radium 226 MDC 0.72 Thorium 230 21 .0 Thorium 230 precision (±) 4.0 Thorium 230 MDC 0.34 Thorium 232 0.67 Thorium 232 precision (±) 0.29 Thorium 232 MDC 0.32 Uranium, Activity 314 CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume 122448000 ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. MDC -Minimum detectable concentration mg/L uCilmL uCilmL uCi/mL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCi/Filter pCiiFilter pCi/Filter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter L MCU Qualifiers RL QCL Method Analysis Date I By 1.5E-10 SW6020 11105116 07:32 I smm 1.0E-16 SW6020 11105116 07:32 I smm E909.0 10126116 07:25 I plj E909.0 10126116 07:25 I plj E909.0 1 0126116 07:25 I plj E903.0 1110711615:37 ldmf E903.0 11107116 15:37 I dmf E903.0 1110711615:37 I dmf E908.0 10126116 17:13 I eng E908.0 10126116 17:13 I eng E908.0 10126116 17:13 I eng E908.0 10126116 17:13 I eng E908.0 10126116 17:13 I eng E908.0 10126116 17:13 I eng RADCALC 1111011613:09 I rdw RADCALC 11110116 13:09 I rdw RADCALC 1111011613:09 I rdw RADCALC 1111011613:09 I rdw RADCALC 11110116 13:09 I rdw RADCALC 11110116 13:09 I rdw RADCALC 11110116 13:09 I rdw RADCALC 1111011613:09 I rdw RADCALC 11110116 13:09 I rdw RADCALC 11127116 12:23 I sec RADCALC 11127116 12:23 I sec RADCALC 11127116 12:23 I sec 0.20 RADCALC 1111011613:091 rdw FIELD 09127116 00:00 I *** MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 13 of 32 EI\ERGY •> ,',I< I' (• Trust our People. Trust our Data. www.energylab.com Toll Free: 888.235.0515 • 307.235.0515 • F: 307.234.1639 PO Box 247, Casper, WY 82602-0247 • 2393 Salt Creek Hwy (82601) HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 3rd Quarter Air 2016 SAMPLE ID: BHV-7 REPORT DATE: November 27, 2016 Quarter/Date Sampled Concentration Air Volume Radionuclide JiCilmL C16100148-006 natu 2.6E-l5 Third Quarter 20 16 23Dn 2E-16 Air Volume in mLs 226Ra 4E-l6 1.22E+11 2IOPb 3E-15 232Th 5E-18 +LLD's are from NRC Reg. Guide 4.14 Counting Precision JJCilmL N/A 3E-l7 SE-17 9E-16 2E-18 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 L.L.D.+ Effluent Cone.* %Effluent MDC JiCilmL JiCilmL JJCilmL Concentration N/A 1E-16 9E-l4 2.8E+00 3E-l8 1E-16 3E-14 6E-OI 6E-l8 IE-16 9E-13 5E-02 2E-16 2E-15 6E-13 5E-Ol 3E-18 N/A 6E-15 9E-02 Page 14 of32 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Lab ID: C17010161-006 Client Sample ID: BHV-7 ---- Analyses Result METALS-IN AIR Uranium 2.4E-09 Uranium, Activity 1.6E-15 RADIONUCLIDES -IN AIR Lead 210 1.5E-14 Lead 210 precision (±) 4.4E-15 Lead 210 MDC 4.6E-16 Radium 226 2.5E-16 Radium 226 precision (±) 5.1E-17 Radium 226 MDC 8.7E-18 Thorium 230 1.2E-16 Thorium 230 precision (±) 2.2E-17 Thorium 230 MDC 2.7E-18 Thorium 232 4.8E-18 Thorium 232 precision (±) 1.7E-18 Thorium 232 MDC 1.6E-18 RADIONUCLIDES -IN AIR -PER FILTER Lead 210 1840 Lead 210 precision(±) 552 Lead 210 MDC 56.6 Radium 226 31.3 Radium 226 precision (±) 6.4 Radium 226 MDC 1.1 Thorium 230 14.4 Thorium 230 precision (±) 2.7 Thorium 230 MDC 0.33 Thorium 232 0.59 Thorium 232 precision (±) 0.21 Thorium 232 MDC 0.20 Uranium, Activity 203 RADIOCHEMISTRY AIR FILTER COMPLIANCE Lead 210,% of EFF Lead 210, EFF Day Lead 210, LLD Radium 226, % of EFF Radium 226, EFF Week Radium 226, LLD Thorium 230, % of EFF Thorium 230, EFF Year Thorium 230, LLD Thorium 232, % of EFF Thorium 232, EFF Year Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. 2.5E+OO 6.0E-13 2.0E-15 3.0E-02 9.0E-13 1.0E-16 3.9E-01 3.0E-14 1.0E-16 8.0E-02 3.0E-14 MDC -Minimum detectable concentration Units mgiL uCilmL uCilmL uCifmL uCilmL uCilmL uCifmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL pCi/Filter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCi/Filter pCi!Filter pCiiFilter pCiiFilter % uCilmL uCilmL % uCilmL uCilmL % uCilmL uCilmL % uCilmL Qualifiers Report Date: 02/03/17 Collection Date: 12/27/16 Date Received: 01/06/17 Matrix: Filter MCU RL QCL Method Analysis Date I By 1.5E-10 SW6020 01127117 19:191 sf 1.0E-16 SW6020 01127117 19:191 sf E909.0 01126117 11 :00 I plj E909.0 01126117 11 :00 I plj E909.0 01126117 11 :00 I plj E903.0 01130117 08:20 I dmf E903.0 01130117 08:20 I dmf E903.0 01130/17 08:20 I dmf E908.0 01124117 09:25 I eng E908.0 01124117 09:251 eng E908.0 01124117 09:251 eng E908.0 01124117 09:25 I eng E908.0 01124117 09:251 eng E908.0 01124117 09:251 eng RADCALC 02103117 15:57 I sec RADCALC 02/03117 15:571 sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02/03117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec 0.20 RADCALC 02103117 15:57 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02/03117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103/17 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:591 sec RADCALC 02103/17 15:591 sec MCL -Maximum contaminant level. NO-Not detected at the reporting limit. Page 18 of 41 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Lab ID: C17010161-006 Client Sample ID: BHV-7 Analyses Result Units RADIOCHEMISTRY AIR FILTER COMPLIANCE Thorium 232, LLD 1.0E-16 Uranium Natural, % of EFF 1.8E+OO Uranium Natural, EFF Year 9.0E-14 Uranium Natural, LLD 1.0E-16 CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. 124298300 uCilml % uCilmL uCilmL L Qualifiers RL MCLI Report Date: 02/03/17 Collection Date: 12/27116 DateReceived: 01/06117 Matrix: Filter QCL Method Analysis Date I By RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec FIELD 12127116 00:00 I*** MCL -Maximum contaminant level. ND-Not detected at the reporting limit. Page 19 of 41 EI\ERGY ,ll > .. 11 11 Trust our People. Trust our Data. www.energylab.com HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc P-ROJECT: 4th Quarter Air 2016 SAMPLE ID: BHV -7 REPORT DATE: February 3, 2017 Quarter/Date Sampled Concentration Radionuclide Air Volume J1CilmL Cl7010161-006 natu 1.6E-15 Fourth Quarter 20 16 23<T!J IE-16 Air Volume in mLs 226Ra 3E-16 1.24E+ll 210Pb 1.5E-14 232Th 5E-18 +LLD's are from NRC Reg. Guide 4.14 Counting Precision 11CilmL N/A 2E-17 5E-17 4E-15 2E-18 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 MDC 11CilmL N/A 3E-18 9E-18 5E-16 2E-18 Billings, MT BOO. 735.4489 • Casper, WY 888.235.0515 Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 L.L.D.+ Effiuent Cone.* % EfOuent J1CilmL 11CilmL Concentration lE-16 9E-14 1.8E+00 IE-16 3E-14 4E-01 IE-16 9E-13 3E-02 2E-15 6E-13 2.5E+00 N/A 6E-15 SE-02 Page 20 of41 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.&90.2218 • Gillette, WY 86&.686.7175 • Helena, MT 817.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2016 Lab ID: C16100148-007 Client Sample ID: BHV-8 Analyses Result Units METALS -IN AIR Uranium 1.7E-09 Uranium, Activity 1.2E-15 RADIONUCLIDES -IN AIR Lead 210 7.6E-15 Lead 210 precision(±) 2.3E-15 Lead 210 MDC 2.6E-16 Radium 226 3.3E-16 Radium 226 precision (±) 6.6E-17 Radium 226 MDC 6.4E-18 Thorium 230 8.4E-17 Thorium 230 precision (±) 1.6E-17 Thorium 230 MDC 3.0E-18 Thorium 232 4.7E-18 Thorium 232 precision (±) 2.1E-18 Thorium 232 MDC 2.4E-18 RADIONUCLIDES -IN AIR -PER FILTER Lead 210 940 Lead 210 precision(±) 281 Lead 210 MDC 31 .9 Radium 226 40.5 Radium 226 precision (±) 8.1 Radium 226 MDC 0.79 Thorium 230 10.3 Thorium 230 precision (±) 2.0 Thorium 230 MDC 0.36 Thorium 232 0.58 Thorium 232 precision (±) 0.26 Thorium 232 MDC 0.29 Uranium, Activity 143 CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume 122971700 *** Field data provided by client Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. MDC -Minimum detectable concentration mgiL uCilmL uCilmL uCilmL uCi/mL uCi/mL uCilmL uCilmL uCi/mL uCilmL uCilmL uCilmL uCilmL uCilmL pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCi/Filter pCi/Filter pCiiFilter pCiiFilter L Qualifiers MCU RL QCL 1.5E-10 1.0E-16 0.20 Report Date: 11/27116 Collection Date: 09/27/16 DateReceived: 10/05/16 Matrix: Filter Method Analysis Date I By SW6020 11105116 07:381 smm SW6020 11105/16 07:381 smm E909.0 10126116 07:58 I plj E909.0 10126116 07:58 I plj E909.0 10126116 07:58 I plj E903.0 11107116 15:37 I dmf E903.0 1110711615:371dmf E903.0 11107116 15:37 I dmf E908.0 10126116 17:131 eng E908.0 10126116 17:131 eng E908.0 10126116 17:131 eng E908.0 10126116 17:131 eng E908.0 10126116 17:13 I eng E908.0 10126116 17:131 eng RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 1111011613:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11110116 13:091 rdw RADCALC 11127116 12:231 sec RADCALC 1112711612:231 sec RADCALC 1112711612:231 sec RADCALC 1111011613:091 rdw FIELD 09127/16 00:00 I*** MCL-Maximum contaminant level. ND -Not detected at the reporting limit. Page 15 of 32 EI\ERGY 1 r '•• ·,•( •I • Trust our People. Trust our Data. www.energylab.com 'I Toll Free: 888.235.0515 • 307.235.0515 • F: 307.234.1639 PO Box 247, Casper, WY 82602-0247 • 2393 Salt Creek Hwy (82601) HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 3rd Quarter Air 2016 SAMPLE ID: BHV -8 REPORT DATE: November 27,2016 Quarter/Date Sampled Concentration Radionuclide Air Volume f.ICilmL Cl6100148-007 ""'U 1.2E-15 Third Quarter 2016 230ojn 8E-17 Air Volume in mLs 226Ra 3E-16 1.23E+ll zwPb 8E-15 232Th SE-18 +LLD's are from NRC Reg. Guide 4.14 Counting Precision f.ICilmL N/A 2E-17 7E-17 2E-15 2E-18 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 L.L.D.+ Effluent Cone.* %Effluent MDCf.ICilmL f.ICilmL f.ICilmL Concentration N/A lE-16 9E-14 1.3E+00 3E-18 IE-16 3E-14 3E-OI 6E-18 IE-16 9E-13 4E-02 3E-16 2E-15 6E-13 IE+OO 2E-18 N/A 6E-15 8E-02 Page 16 of 32 EN:RGY ; Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Lab ID: C17010161-007 Client Sample ID: BHV-8 ------ Analyses Result METALS -IN AIR Uranium 1.8E-09 Uranium, Activity 1.2E-15 RADIONUCLIDES -IN AIR Lead 210 1.4E-14 Lead 210 precision(±) 4.3E-15 Lead 210 MDC 4.6E-16 Radium 226 8.5E-17 Radium 226 precision (±) 2.1 E-17 Radium 226 MDC 8.8E-18 Thorium 230 6.0E-17 Thorium 230 precision (±) 1.1E-17 Thorium 230 MDC 1.8E-18 Thorium 232 3.2E-18 Thorium 232 precision (±) 1.3E-18 Thorium 232 MDC 1.4E-18 RADIONUCLIDES -IN AIR -PER FILTER Lead 210 1720 Lead 210 precision (±) 515 Lead 210 MDC 55.0 Radium 226 10.2 Radium 226 precision (±) 2.5 Radium 226 MDC 1.1 Thorium 230 7.2 Thorium 230 precision (±) 1.4 Thorium 230 MDC 0.22 Thorium 232 0.38 Thorium 232 precision (±) 0.16 Thorium 232 MDC 0.16 Uranium, Activity 145 RADIOCHEMISTRY AIR FILTER COMPLIANCE Lead 210, %of EFF Lead 210, EFF Day Lead 210, LLD Radium 226, % of EFF Radium 226, EFF Week Radium 226, LLD Thorium 230, % of EFF Thorium 230, EFF Year Thorium 230, LLD Thorium 232, % of EFF Thorium 232, EFF Year Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. 2.4E+OO 6.0E-13 2.0E-15 9.0E-03 9.0E-13 1.0E-16 2.0E-01 3.0E-14 1.0E-16 5.0E-02 3.0E-14 MDC -Minimum detectable concentration Units mgll uCilml uCilml uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL uCilmL pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCiiFilter pCi/Filter pCiiFilter pCiiFilter % uCilml uCilmL % uCilmL uCilmL % uCilmL uCilmL % uCilmL Report Date: 02/03/17 Collection Date: 12/27/16 DateReceived: 01/06/17 Matrix: Filter MCU Qualifiers RL QCL Method Analysis Date I By 1.5E-10 SW6020 01127117 19:22 I sf 1.0E-16 SW6020 01127117 19:22 I sf E909.0 01126117 11:13 I plj E909.0 01126117 11:13 I plj E909.0 0112611711:131 plj E903.0 01130117 08:20 I dmf E903.0 01130117 08:20 I dmf E903.0 01130117 08:20 I dmf E908.0 01124117 09:25 I eng E908.0 01124117 09:25 I eng E908.0 01124117 09:25 I eng E908.0 01124117 09:25 I eng E908.0 01124117 09:25 I eng E908.0 01124117 09:25 I eng RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:571 sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec 0.20 RADCALC 02103117 15:57 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 21 of 41 EI\ERGY Trust our People. Trust our Data. www.energ ylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Lab ID: C17010161-007 Client Sample ID: BHV-8 ----------------- Analyses Result Units RADIOCHEMISTRY AIR FILTER COMPLIANCE Thorium 232, LLD 1.0E-16 Uranium Natural, % of EFF 1.3E+OO Uranium Natural, EFF Year 9.0E-14 Uranium Natural, LLD 1.0E-16 CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume *** Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. 120089800 uCilmL % uCi/mL uCilmL L Qualifiers RL MCU Report Date: 02/03/17 Collection Date: 12/27116 DateReceived: 01/06/17 Matrix: Filter QCL Method Analysis Date I By RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec FIELD 12127116 00:00 I ••• MCL-Maximum contaminant level. ND-Not detected at the reporting limit. Page 22 of 41 EI\ERGY ,,, ' " Trust our People. Trust our Data. www.energylab.com HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 4th Quarter Air 2016 SAMPLE ID: BHV-8 REPORT DATE: February 3, 2017 Quarterillate Sampled Concentration Air Volume Radionuclide J1CilmL c 17010161-007 ""u l.2E-15 Fourth Quarter 20 16 23Dn 6E-17 Air Volume in mLs 226Ra 8E-17 l.20E+11 2JOPb l.4E-14 231n 3E-18 +LLD's are from NRC Reg. Guide 4.14 Counting Precision J1CilmL N/A IE-17 2E-17 4E-15 1E-18 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 MDCJ1CilmL N/A 2E-18 9E-18 SE-16 IE-18 Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 L.L.D.+ Eflluent Cone.* %Effluent J!CilmL J1CilmL Concentration 1E-16 9E-14 1.3E+00 IE-16 3E-14 2E-Ol lE-16 9E-13 9E-03 2E-15 6E-13 2.4E+00 N/A 6E-15 SE-02 Page 23 of 41 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LAB ORA TORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2016 Lab ID: C16100148-008 Client Sample ID: Blanks Analyses METALS -IN AIR Uranium Uranium, Activity RADIONUCLIDES -IN AIR Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC RADIONUCLIDES -IN AIR-PER FILTER Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Uranium, Activity CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.0031 mgiL 2.1 E-09 uCilmL -5.5E-10 uCilmL 3.8E-09 uCilmL 6.4E-09 uCilmL 9.2E-10 uCilmL 6.4E-10 uCilmL 7.9E-10 uCilmL 5.5E-10 uCilmL 3.6E-1 0 uCilmL 5.3E-10 uCi/mL 9.9E-11 uCilmL 2.7E-1 0 uCilmL 5.0E-10 uCi/mL -0.55 pCiiFilter 3.8 pCi/Filter 6.4 pCiiFilter 0.92 pCi!Filter 0.64 pCi/Filter 0.79 pCiiFilter 0.55 pCiiFilter 0.36 pCi!Filter 0.53 pCi/Filter 0.099 pCi/Filter 0.27 pCi!Filter 0.50 pCi/Filter 2.1 pCi/Filter 1 L MDC -Minimum detectable concentration Qualifiers D D u u u u U -Not detected at minimum detectable concentration MCU RL QCL 8.5E-06 5.8E-12 0.20 Report Date: 11/27116 Collection Date: 09/27/16 Date Received: 10/05/16 Matrix: Filter Method Analysis Date I By SW6020 11105116 07:44 I smm SW6020 11105116 07:44 I smm E909.0 10126116 00:24 I eli-cs E909.0 10126116 00:24 I eli-cs E909.0 10126116 00:24 I eli-cs E903.0 11107116 15:37 I dmf E903.0 11107116 15:37 I dmf E903.0 11107116 15:37 I dmf E908.0 10126116 17:13 I eng E908.0 10126116 17:13 I eng E908.0 1012611617:13 I eng E908.0 10126116 17:13 I eng E908.0 1012611617:13 I eng E908.0 10126116 17:13 I eng RADCALC 11/27116 10:48 I sec RADCALC 11127116 10:48 I sec RADCALC 1112711610:48 I sec RADCALC 11/27/16 10:48/ sec RADCALC 11/27116 10:48 I sec RADCALC 11127/16 10:48/ sec RADCALC 11127116 10:48 I sec RADCALC 11127/16 10:48/ sec RADCALC 11127116 10:48 I sec RADCALC 11127116 12:23 I sec RADCALC 11127/16 12:23 I sec RADCALC 11127/16 12:23/ sec RADCALC 11/27116 10:48 I sec FIELD 09127116 00:00 I*** MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 17 of 32 EN:RGY l.r •• I ' 1 Trust our People. Trust our Data. www.energylab.com Toll Free: 888.235.0515 o 307.235.0515 o F: 307.234.1639 PO Box 247, Casper, WY 82602-0247 o 2393 Salt Creek Hwy (82601) HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 3rd Quarter Air 2016 SAMPLE ID: Blanks REPORT DATE: November 27,2016 Quarter/Date Sampled Concentration Radionuclide Air Volume J!CilmL c 16100148-008 nalu 2E-17 Third Quarter 20 16 23~ 4E-18 Air Volume in mLs 226Ra 7E-18 1.36E+11 210Pb -4E-18 232Th 7E-19 Counting L.L.D.+ Precision MDC pCilmL pCilmL pCi/mL N/A N/A IE-16 3E-1 8 4E-18 1E-16 SE-18 6E-18 1E-16 3E-17 SE-17 2E-15 2E-18 4E-18 N/A NOTE: This report uses 136,000,000 Lair for comparison purposes, the routme report uses a 1 L system default. +LLD's are from NRC Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 Effluent Cone.* %Effluent pCilmL Concentration 9E-14 2E-02 3E-14 1E-02 9E-13 8E-04 6E-13 -7E-04 6E-15 lE-02 Page 18 of 32 Er\ERGY .· Trust our People. Trust our Data. www.energylab com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.&90.2218 • Gillette, WY 866.&86.7175 • Helena, MT 877.472.0711 LAB ORA TORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Lab ID: C17010161-008 Client Sample ID: Blanks Analyses Result Units Qualifiers METALS-IN AIR Uranium 0.0018 mgiL D Uranium, Activity 1.2E-09 uCilml D RADIONUCLJDES -IN AIR Lead 210 2.9E-09 uCilmL u Lead 210 precision(±) 8.4E-09 uCi/ml Lead 210 MDC 1.4E-08 uCilmL Radium 226 1.1E-09 uCilmL Radium 226 precision (±) 7.2E-10 uCilmL Radium 226 MDC 1.1E-09 uCilmL Thorium 230 1.8E-09 uCilmL Thorium 230 precision (±) 3.4E-10 uCilmL Thorium 230 MDC 8.7E-10 uCilmL Thorium 232 2.0E-10 uCilmL Thorium 232 precision (±) 1.3E-10 uCilmL Thorium 232 MDC 1.9E-1 0 uCilmL RADIONUCLJDES -IN AIR-PER FILTER Lead 210 2.9 pCiiFilter u Lead 210 precision (±) 8.4 pCiiFilter Lead 210 MDC 14.0 pCiiFilter Radium 226 1.1 pCiiFilter Radium 226 precision (±) 0.72 pCiiFilter Radium 226 MDC 1.1 pCiiFilter Thorium 230 1.8 pCiiFilter Thorium 230 precision (±) 0.34 pCi!Filter Thorium 230 MDC 0.87 pCiiFilter Thorium 232 0.20 pCiiFilter Thorium 232 precision (±) 0.13 pCi/Filter Thorium 232 MDC 0.19 pCi/Filter Uranium, Activity 1.2 pCiiFilter RADIOCHEMISTRY AIR FILTER COMPLIANCE Lead 210,% of EFF 4.8E+05 % Lead 210, EFF Day 6.0E-13 uCilmL Lead 210, LLD 2.0E-15 uCilmL Radium 226, % of EFF 1.2E+05 % Radium 226, EFF Week 9.0E-13 uCilmL Radium 226, LLD 1.0E-16 uCilmL Thorium 230, % of EFF 6.0E+06 % Thorium 230, EFF Year 3.0E-14 uCilmL Thorium 230, LLD 1.0E-16 uCilmL Thorium 232, % of EFF 3.3E+06 % Thorium 232, EFF Year 3.0E-14 uCilmL Report RL -Analyte reporting limit. Definitions: QCL -Quality control limit. MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration MCU RL QCL 0.000030 2.0E-11 0.20 Report Date: 02/03/17 Collection Date: 12/27116 DateReceived: 01/06/17 Matrix: Filter Method Analysis Date I By SW6020 01127117 19:241 sf SW6020 01127117 19:241 sf E909.0 01126117 11:261 plj E909.0 01126117 11 :26 I plj E909.0 01126117 11 :26 I plj E903.0 01130117 08:20 I dmf E903.0 01130117 08:20 I dmf E903.0 01130117 08:20 I dmf E908.0 01124117 09:251 eng E908.0 01124117 09:251 eng E908.0 01124117 09:251 eng E908.0 01124117 09:251 eng E908.0 01124117 09:251 eng E908.0 01124117 09:25 I eng RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:571 sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:571 sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:57 I sec RADCALC 02103117 15:571 sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:591 sec RADCALC 02103117 15:59 I sec RADCALC 02103117 15:591 sec MCL -Maximum contaminant level. NO -Not detected at the reporting limit. D-RL increased due to sample matrix. Page 24 of 41 Er\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT BOO. 735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Lab ID: C17010161-008 Client Sample ID: Blanks Report Date: 02/03/17 Collection Date: 12/27/16 DateReceived: 01/06/17 Matrix: Filter ------------------ Analyses Result Units RADIOCHEMISTRY AIR FILTER COMPLIANCE Thorium 232, LLD Uranium Natural, % of EFF Uranium Natural, EFF Year Uranium Natural, LLD CLIENT PROVIDED FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. 1 .OE-16 uCi/mL 1.4E+06 % 9.0E-14 uCi/mL 1.0E-16 uCilmL 1 L Qualifiers RL MCU QCL Method RADCALC RADCALC RADCALC RADCALC FIELD MCL-Maximum contaminant level. Analysis Date I By 02103117 15:591 sec 02/03117 15:59 I sec 02103117 15:59 I sec 02103117 15:59 I sec 12127116 00:00 I ••• NO -Not detected at the reporting limit. Page 25 of41 EI\ERGY , • ',•, '•I • I I Trust our People. Trust our Data. www.energylab.com HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc PROJECT: 4th Quarter Air 2016 SAMPLE ID: Blanks REPORT DATE: February 3, 2017 Quarterillate Sampled Concentration Radionuclide Air Volume 11CilmL Cl7010161-008 ""'U 9E-18 Fourth Quarter 2016 23~ IE-17 Air Volume in mLs 226Ra 8E-18 1.36E+ll 210Pb 2E-17 232-yh IE-18 Counting Precision MDC 11CilmL 11CilmL N/A N/A 3E-18 6E-18 5E-18 SE-18 6E-17 IE-16 IE-18 IE-18 Billings, MT BOO. 735.4489 • Casper, WY 888.235.0515 Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 L.L.D.+ Effluent Cone.* %Effluent 11CilmL 11CilmL Concentration IE-16 9E-14 IE-02 IE-16 3E-14 4E-02 IE-16 9E-13 9E-04 2E-15 6E-13 4E-03 N/A 6E-15 2E-02 NOTE: This report uses 136,000,000 L a1r for companson purposes, the routme report uses a 1 L system default. +LLD's are from NRC Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230, Thorium-232 Week for Radium-226 Day for Lead-210 Page 26 of41 EI\ERGY Trust our People. Trust our Dati. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7115 • Helena, MT 877.472.0711 November 27, 2016 Energy Fuels Resources (USA) Inc 225 Union Blvd Ste 600 Lakewood, CO 80228-1826 Work Order: C16100148 ANALYTICAL SUMMARY REPORT Project Name: 3rd Quarter Air 2016 Energy Laboratories, Inc. Casper WY received the following 8 samples for Energy Fuels Resources (USA) Inc on 10/5/2016 for analysis. LabiD Client Sample ID Collect Date Receive Date Matrix Test C161 00148-001 BHV-1 09/27/16 00:00 10/05/16 Filter Composite of two or more samples Client Provided Field Parameters Metals, Total Digestion, Total Metals, Radiochemistry Radiochemistry Air Filter Compliance Calculations RAD-AIR, Routine Radiological Reports RAD Alternate Unit Reporting Air Filters Lead 210 Radium 226 Thorium, Isotopic C16100148-002 BHV-2 09/27/16 00:00 10/05/16 Filter Same As Above C16100148-003 BHV-4 09/27/16 00:00 10/05/16 Filter Same As Above C16100148-004 BHV-5 09/27/16 00:00 10/05/16 Filter Same As Above C161 00148-005 BHV-6 09/27/16 00:00 10/05/16 Filter Same As Above C16100148-006 BHV-7 09/27/16 00:00 10/05/16 Filter Same As Above C16100148-007 BHV-8 09/27/16 00:00 10/05/16 Filter Same As Above c 16100148-008 Blanks 09/27/16 00:00 10/05/16 Filter Same As Above The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: Digitally signed by Steve Carlston Date: 2016.11.27 13:14:43 -07:00 Page 1 of 32 Er\ERGY Trust our People. Trust our Data. www.ene rgyl ab.co m Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Collage Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 CLIENT: Project: Work Order: Energy Fuels Resources (USA) Inc 3rd Quarter Air 2016 C16100148 BRANCH LABORATORY SUBCONTRACT ANALYSIS Report Date: 11/27/16 CASE NARRATIVE Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4°C (±2°C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g-Energy Laboratories, Inc.-Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-cs-Energy Laboratories, Inc.-College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641 , Radiochemical E871 017; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted f()r regulatory enforcement should be certified in the sample state of origin. Please verify Ell's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 32 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2016 Analyte Count Result Units Method: E903.0 Lab ID: C16100300-001AMS Radium 226 Lab ID: C161 00300-001 AMSD Radium 226 Lab ID: LCS-48516 Radium 226 Lab ID: MB-48516 Radium 226 Radium 226 precision (±) Radium 226 MDC Qualifiers: RL-Analyte reporting limit. 3 MDC -Minimum detectable concentration Sample Matrix Spike 109 pCi/L Sample Matrix Spike Duplicate 127 pCi/L Laboratory Control Sample 19.7 pCi/L Method Blank 0.2 pCi/L 0.2 pCi/L 0.2 pCi/L Report Date: 11/27/16 Work Order: C16100148 RL %REC Low Limit High Limit RPD RPDLimit Qual Run: TENNELEC-3_161 028A 80 70 130 Run: TENNELEC-3_161 028A ~ ro 1~ 15 Run: TENNELEC-3_161 028A 100 80 120 Run: TENNELEC-3_161 028A ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: 48516 11/07/16 15:37 11/07/16 15:37 20 11/07/16 15:37 11/07/16 15:37 u Page 19 of 32 EN:RGY ' •' Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2016 Analyte Count Result Units Method: E908.0 Lab ID: LCS-48356 Thorium 230 LabiD: C16100148-007AMS Thorium 230 LabiD: C16100148-007AMSD Thorium 230 Lab ID: MB-48516 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC LabiD: MB-48356 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Qualifiers: RL-Analyte reporting limit. 6 6 MDC -Minimum detectable concentration Laboratory Control Sample 24.8 pCi/L Sample Matrix Spike 4.67E-07 pCi/L Sample Matrix Spike Duplicate 5.30E-07 pCi/L Method Blank 0.3 pCi/L 0.7 pCi/L 1 pCi/L -0.02 pCi/L 0.09 pCi/L 0.2 pCi/L Method Blank 0.3 pCi/L 0.2 pCi/L 0.3 pCi/L 0.02 pCi/L 0.08 pCi/L 0.2 pCi/L Report Date: 11/27116 Work Order: C16100148 RL %REC Low Limit High Limit RPD RPDLimit Qual Batch: A48356-48516 Run: EGG-ORTEC_161017B 103 80 120 Run: EGG-ORTEC_161017B 99 70 130 Run: EGG-ORTEC_161017B 115 70 130 13 Run : EGG-ORTEC_161017B Run: EGG-ORTEC_161017B NO-Not detected at the reporting limit. U -Not detected at minimum detectable concentration 10/26/16 17:13 10/26/16 17:13 10/26/16 17:13 20 10/26/16 17:13 u u 10/27/16 10:02 u u Page 20 of 32 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 886.686.7175 • Helena, MT 871.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2016 Analyte Method: E909.0 Lab ID: LCS-PB-210-0794 Lead 210 Lab ID: MB-48516 Lead 210 Lead 21 0 precision (±) Lead 210 MDC Lab ID: C16100300-002AMS Lead 210 Lab ID: C16100300-002AMSD Lead 210 Method: E909.0 Lab ID: MB-25645 Lead 210 Lead 210 precision (±) Lead 210 MDC Lab 10: LCS-25645 Lead 210 Lab ID: C16100148-001A Lead 210 Lab 10: C16100148-001A Lead 210 Count Result Units Laboratory Control Sample 64.2 pCi/L 3 Method Blank -0.3 pCi/L 0.8 pCi/L pCi/L Sample Matrix Spike 3340 pCi/L Sample Matrix Spike Duplicate 3020 pCi/L 3 Method Blank 1.0 pCi/L 4 pCi/L 6 pCi/L Laboratory Control Sample 61 .1 pCi/L Sample Matrix Spike 1.45E-05 pCi/L Sample Matrix Spike Duplicate 1.48E-05 pCi/L Report Date: 11/27/16 Work Order: C16100148 RL %REC Low Limit High Limit RPD RPDLimit Qual Run : PACKARD 3100TR_161020A 80 70 130 Run : PACKARD 3100TR_161020A Run: PACKARD 3100TR_161020A 90 70 130 Run: PACKARD 3100TR_161020A n ro 1~ 10 Run: SUB-T70140 Run: SUB-T70140 100 80 120 Run: SUB-T70140 123 70 130 Run: SUB-T70140 142 70 130 2.5 Batch: PB-210-0794 10/25/16 13:17 10/25/16 13:50 u 10/26/16 08:38 10/26/16 08:4 7 20 Batch: T _25645 10/25/16 19:16 u 1 0/25/16 20:59 1 0/25/16 22:50 10/25/16 23:12 69.1 s -Sample activity for this radionuclide is much larger than the spike activity added. Therefore the matrix spike recovery could not be calculated. The LCS and the RPD of the MS/MSD pair are acceptable; this batch is approved. Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits. U -Not detected at minimum detectable concentration Page 21 of 32 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2016 Analyte Count Result Units Method: SW6020 LabiD: MB-48516 Method Blank Uranium 0.0002 mg/L LabiD: LCS2-48516 Laboratory Control Sample Uranium 0.102 mg/L Lab ID: C161 00300-001 ADIL Serial Dilution Uranium 2.08E-10 mg/L Method: SW6020 LabiD: ICSA Interference Check Sample A Uranium 4.83E-05 mg/L LabiD: ICSAB Interference Check Sample AB Uranium -4.40E-05 mg/L RL 3E-05 8.5E-06 1.5E-10 0.00030 0.00030 Report Date: 11/27/16 Work Order: C16100148 %REC Low Limit High Limit RPD RPDLimit Qual Batch: 48516 Run: ICPMS4-C_161031A 11/02/16 01 :50 Run: ICPMS4-C_161031A 11/02/16 01 :57 101 85 115 Run: ICPMS4-C_161031A 11/02/16 02:15 20 N Analytical Run: ICPMS4-C_1611 04A 11/04/16 17:23 11/04/16 17:29 LabiD: ICV Initial Calibration Verification Standard 11/05/16 05:27 Uranium 0.0455 mg/L Method: SW6020 Lab ID: MB-48516 Method Blank Uranium 4E-05 mg/L LabiD: C161 00300-001 ADIL Serial Dilution Uranium 2.16E-10 mg/L LabiD: C161 00148-008AMS Sample Matrix Spike Uranium 0.0657 mg/L Lab ID: C161 00148-008AMSD Sample Matrix Spike Duplicate Uranium 0.0649 mg/L Qualifiers: RL-Analyte reporting limit. MDC -Minimum detectable concentration 0.00030 91 90 110 Batch: 48516 Run: ICPMS4-C_161104A 11/05/16 05:59 3E-05 Run: ICPMS4-C_161104A 11/05/16 06:24 1.5E-10 20 N Run: ICPMS4-C_161104A 11/05/16 07:50 8.5E-06 125 75 125 Run: ICPMS4-C_161104A 11/05/16 07:56 8.5E-06 124 75 125 1.1 20 NO-Not detected at the reporting limit. N -The analyte concentration was not sufficiently high to calculate a RPD for the serial dilution test. Page 22 of32 EI\ERGY Trust our People. Trust our Data. WI'IW.energylab com Billings, MT 800.735.4489 o Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7175 o Helena, MT 877.472.0711 Work Order Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Tessa Parke Reviewed by: Terry Friedlan Reviewed Date: 10/7/2016 Shipping container/cooler in good condition? Custody seals intact on all shipping container(s)/cooler(s)? Custody seals intact on all sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res Cl, Sulfite, etc.) Temp Blank received in all shipping container(s)/cooler(s)? Container/Temp Blank temperature: Water-VOA vials have zero heads pace? Water-pH acceptable upon receipt? Standard Reporting Procedures: Yes 0 Yes D Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes D ·c Yes D Yes D C16100148 Date Received: 10/5/2016 Received by: tjp NoD NoD NoD NoD NoD NoD NoD No 0 NoD NoD NoD NoD NoD Carrier name: Ground Not Present D Not Present 0 Not Present 0 Not Applicable 0 Not Applicable 0 Not Applicable 0 Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Contact and Corrective Action Comments: None Page 23 of 32 Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: Energy Laboraties Contact: Garrin Palmer ~2~39~3~S~a~lt~C~r-e~ek~H~wy--.--------------Ph:4356782221 Casper WY, 82601 qpalmer@energyfuels.com Chain of Custody/Sampling Analysis Request Project Samplers Name Samplers Signature 3rd Quarter Air 2016 Garrin Palmer I {:,..~-~ Time SampleiD Date Collected Collected Laboratory Analysis Requested BHV-1 6/27/16-9/27116 NA U-NAT, TH-230, Ra-226, Pb-210, TH-232 BHV-2 6/27/16-9/27/16 NA U-NAT, TH-230, Ra-226, Pb-210, TH-232 BHV-4 6/27116-9/27116 NA U-NAT. TH-230, Ra-226, Pb-210, TH-232 BHV-5 6/27/16 -9/27/16 NA U-NAT, TH-230, Ra-226, Pb-210, TH-232 BHV-6 6/27/16-9/27/16 NA U-NAT, TH-230, Ra-226, Pb-210, TH-232 BHV-7 6/27/16-9/27/16 NA U-NAT, TH-230, Ra-226, Pb-210, TH-232 BHV-8 6/27/16. 9/27/16 NA U-NAT, TH-230, Ra-226, Pb-210, TH-232 Blanks 6/27/16-9/27/16 NA U-NAT, TH-230, Ra-226, Pb-210, TH-232 Comments: Please send re_port to Kathy Weinel at kweinel@energyfuels.com Relinquished By:(Signature) "TC/1/..,_-~ Date/Time Received By:(Signature) lli/'3 ttj/ /'l,o, Datemme Page 2 4 a'32 •·o :;. ...... · m= 11.5008 ~:"·~·~~. ; .. ~:';~~~_·::z~-:r. r~ ~-~··,"t.\..-a'-\l: -~ ~ '15 ~ Q) a ., IJ._ a. ... :, ........ -pg,~"f~~·~ .. ~~ \,'(nt',~o.0'4'.,.,...,~.. ~ •• _r .... -,..,~,.,,liJII..:'":":'~":•"'•··· ... J.:·: • ~.tt ... j;....;d,r~Ni:.r,, . ; ... _,.-.... 111 =·-·n~~<" ·;··· .. Period: June 27th, 2016 - , June 27th, '"fi-r-~, .• 8 . ,SA;.}Etf ~;.1 ;:a,,~~~ ·:;':';S'{~~tili1..c.r.~~t{; 5 2016 Week Filter ·start Stop Net # Number Date Date 1 9219790 27-Jun-16 05-Jul-16 4.3648 2 9219782 05-Jul-16 11-Jul-16 4.3795 3 9219781 11-Jul-16 18-Jul-16 4.3799 4 9219766 18-Jul-16 25-Jul-16 4.3621 5 9219765 25-Jul-16 01-Aug-16 4.3598 6 9219750 01-Aug-16 08-Aug-16 4.3889 7 9219749 08-Aug-16 15-Aug-16 4.3762 B 9219734 15-Aug-16 22-Aug-16 4.3078 9 9219733 22-Al!Q-16 29-Au_g_-16 4.3572 10 9219718 29-A(!g-16 06-Sej)_-16 4.3755 11 9219717 06-Sep-16 12-Sep-16 4.3829 12 9219702 12-Sep-16 19-Sep-16 4.3674 13 9219701 19-SeQ-16 27 -SE!Q_-16 4.3999 Totals Page 32 at 32 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.412.0711 February 03, 2017 Energy Fuels Resources (USA) Inc 225 Union Blvd Ste 600 Lakewood, CO 80228-1826 Work Order: C17010161 ANALYTICAL SUMMARY REPORT Quote ID: C4886 -Quarterly Air Analysis Project Name: 4th Quarter Air 2016 Energy Laboratories, Inc. Casper WY received the following 8 samples for Energy Fuels Resources (USA) Inc on 1/6/2017 for analysis. LabiD Client Sample ID Collect Date Receive Date Matrix Test C17010161-001 BHV-1 12/27/16 00:00 01/06/17 Filter Composite of two or more samples Client Provided Field Parameters Metals, Total Digestion, Total Metals, Radiochemistry Radiochemistry Air Filter Compliance Calculations RAD-AIR, Routine Radiological Reports RAD Alternate Unit Reporting Air Filters Lead 210 Radium 226 Thorium, Isotopic C17010161-002 BHV-2 12/27/16 00:00 01/06/17 Filter Same As Above C17010161-003 BHV-4 12/27116 00:00 01/06/17 Filter Same As Above C17010161-004 BHV-5 12/27/16 00:00 01/06/17 Filter Same As Above C17010161-005 BHV-6 12/27116 00:00 01/06/17 Filter Same As Above C1701 0161-006 BHV-7 12/27116 00:00 01/06/17 Filter Same As Above C1701 0161-007 BHV-8 12/27/16 00:00 01/06/17 Filter Same As Above C17010161-008 Blanks 12/27116 00:00 01/06/17 Filter Same As Above The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: AU0tt~ I Project Specialist Digitally signed by Steve Carlston Date: 2017.02.05 12:36:37-07:00 Page 1 of41 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 CLIENT: Project: Work Order: Energy Fuels Resources (USA) Inc 4th Quarter Air 2016 C17010161 ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4°C (±2°C) Report Date: 02/03/17 CASE NARRATIVE Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediatel y after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g-Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT CERTIFICATIONS: USEPA: WY00002; FL-DOH NELAC: E87641; Oregon: WY200001; Utah: WY00002; Washington: C1012 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC .-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify Ell's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 41 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.071 t QAIQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Analyte Count Result Units Method: E903.0 Lab ID: LCS-49035 Radium 226 Lab ID: MB-49035 Radium 226 Radium 226 precision (±) Radium 226 MDC Lab ID: C1701 0178-001 AMS Radium 226 Lab ID: C17010178-001AMSD Radium 226 Qualifiers: RL -Analyte reporting limit. Laboratory Control Sample 72.9 pCi/L 3 Method Blank 0.05 pCi/L 0.2 pCi/L 0.3 pCi/L Sample Matrix Spike 138 pCi/L Sample Matrix Spike Duplicate 137 pCi/L MDC -Minimum detectable concentration Report Date: 02/03/17 Work Order: C17010161 RL %REC Low Limit High Limit Run: G542M_170120A 118 80 120 Run: G542M_170120A Run:G542M_170120A 98 70 130 Run:G542M_170120A 98 70 130 NO -Not detected at the reporting limit. RPD RPDLimit Qual 0.1 Batch: R_219418 01/30/17 08:20 01/30/17 08:20 u 01/30/17 08:20 01/30/1710:11 20 U -Not detected at minimum detectable concentration Page 27 of 41 EN:RGY Trust our People. Trust our Data. www.energylab.com -------' Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 888.888.7175 • Helena, MT 877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Analyte Count Result Units Method: E908.0 Lab 10: LCS-49035 Thorium 230 Lab 10: C17010124-001AMS Thorium 230 Lab 10: C17010124-001AMSO Thorium 230 LabiO: MB-49035 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Qualifiers: RL -Analyte reporting limit. 6 MDC -Minimum detectable concentration Laboratory Control Sample 51.0 pCi/L Sample Matrix Spike 113 pCi/L Sample Matrix Spike Duplicate 107 pCi/L Method Blank 0.6 pCi/L 0.5 pCi/L 0.9 pCi/L 0.1 pCi/L 0.1 pCi/L 0.2 pCi/L Report Date: 02/03/17 Work Order: C17010161 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: EGG-ORTEC_2_170117A 105 80 120 Run: EGG-ORTEC_2_170117A 113 70 130 Run: EGG-ORTEC_2_170117A 107 70 130 5.1 Run: EGG-ORTEC_2_170117A ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: 49035 01/24/17 09:25 01/24/17 09:25 01/24/17 09:25 20 01/24/17 09:24 u u Page 28 of41 Er\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WV 866.686.7175 • Helena, MT 817.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Analyte Count Result Units Method: Lab ID: Lead 210 E909.0 LCS-49035 Lab 10: MB-49035 Lead 210 Lead 210 precision (±) Lead 210 MDC Lab ID: C17010092-001AMS Lead 210 Lab ID: C17010092-001AMSD Lead 210 Qualifiers: RL -Analyte reporting limit. Laboratory Control Sample 34.9 pCi/L 3 Method Blank 0.3 pCi/L pCi/L 2 pCi/L Sample Matrix Spike 401 pCi/L Sample Matrix Spike Duplicate 389 pCi/L MDC -Minimum detectable concentration Report Date: 02/03/17 Work Order: C17010161 RL %REC Low Limit High Limit RPD RPDLimit Qual Run: PACKARD 3100TR_170120A 114 70 130 Run: PACKARD 3100TR_170120A Run: PACKARD 3100TR_170120A 104 70 130 Run: PACKARD 3100TR_170120A 101 70 130 2.9 ND -Not detected at the reporting limit. Batch: PB-210-0808 01/25/17 14:28 01/25/17 15:41 u 01/26/17 01:42 01/26/17 02:47 20 U -Not detected at minimum detectable concentration Page 29 of 41 EI\ERGY Trust our People. Trust our Data. www.e ne 1gylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2016 Analyte Count Result Method: SW6020 Units RL %REC Low Limit Report Date: 02/03/17 Work Order: C17010161 High Limit RPD RPDLimit Qual Analytical Run: ICPMS4-C_170117B LabiD: ICV Initial Calibration Verification Standard 01/17/1716:38 Uranium 0.0479 mg/L 0.00030 96 90 110 Lab ID: ICSA Interference Check Sample A 01/17/17 16:41 Uranium 7.43E-05 mg/L 0.00030 LabiD: ICSAB Interference Check Sample AB 01/17/17 16:43 Uranium 6.50E-06 mg/L 0.00030 Method: SW6020 Batch: 49035 Lab ID: MB-49035 Method Blank Run: ICPMS4-C_170117B 01/17/17 17:23 Uranium NO mg/L 3E-05 Lab ID: LCS2-49035 Laboratory Control Sample Run: ICPMS4-C_170117B 01/17/17 17:26 Uranium 0.0915 mg/L 3.0E-05 92 85 115 LabiD: C1701 0161-00BAMS Sample Matrix Spike Run: ICPMS4-C_170117B 01/17/1718:14 Uranium 0.0538 mg/L 3.0E-05 104 75 125 LabiD: C1701 0161-00BAMSD Sample Matrix Spike Duplicate Run: ICPMS4-C_170117B 01/17/1718:16 Uranium 0.0541 mg/L 3.0E-05 105 75 125 0.7 20 Method: SW6020 Batch: 49035 LabiD: C17010161-008AMS Sample Matrix Spike Run: ICPMS4-C_170125B 01/26/17 17:38 Uranium 0.0576 mg/L 3.0E-05 111 75 125 LabiD: C1701 0161-00SAMSD Sample Matrix Spike Duplicate Run: ICPMS4-C_170125B 01/26/17 17:41 Uranium 0.0568 mg/L 3.0E-05 110 75 125 1.4 20 Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration Page 30 of41 EN:RGY •' Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Collep Station, TX 888.890.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 02/03/17 Work Order: C17010161 Project: 4th Quarter Air 2016 Analyte Count Result Units RL o/oREC Low Limit High Limit RPD RPDLimit Qual Method: SW6020 Lab ID: ICV Uranium Lab ID: ICSA Uranium Lab ID: ICSAB Uranium Method: LabiD: Uranium SW6020 MB-49035 Lab ID: LCS2-49035 Uranium Lab ID: C17010161-001AMS Uranium Lab ID: C17010161-001AMSD Uranium Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Initial Calibration Verification Standard 0.0489 mg/L 0.00030 Interference Check Sample A -2.00E-07 mg/L 0.00030 Interference Check Sample AB -2.80E-06 mg/L 0.00030 Method Blank 4E-05 mg/L 3E-05 Laboratory Control Sample 0.0945 mg/L 3.0E-05 Sample Matrix Spike 3.48E-09 mg/L 1.5E-1 0 Sample Matrix Spike Duplicate 3.48E-09 mg/L 1.5E-10 Analytical Run: ICPMS4-C_170127C 01/27/17 18:15 98 90 110 Run: ICPMS4-C_170127C Run: ICPMS4-C_170127C 94 85 115 Run: ICPMS4-C_170127C 101 75 125 Run: ICPMS4-C_170127C 101 75 125 0.0 01/27/17 18:27 01/27/17 18:30 Batch: 49035 01/27/17 18:45 01/27/17 18:47 01/27/17 18:57 01/27/17 18:59 20 NO -Not detected at the reporting limit. Page 31 of 41 EN:RGY Trust our People. Trust our Data. www.energylab.com Work Order Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Corinne Wagner Reviewed by: Kasey Vidick Reviewed Date: 1/9/2017 Shipping container/cooler in good condition? Custody seals intact on all shipping container(s)/cooler(s)? Custody seals intact on all sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH , DO, Res Cl, Sulfite, Ferrous Iron, etc.) Temp Blank received in all shipping container(s)/cooler(s)? Container/Temp Blank temperature: Water-VOA vials have zero headspace? Water-pH acceptable upon receipt? Standard Reporting Procedures: Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes D Yes D Yes D Billings, MT 800.735.4489 o Casper, WY 888.235.0515 Gillette, WY 888.686.7175 o Helena, MT 877.472.0711 C17010161 Date Received: 1/6/2017 Received by: ckw Carrier name: NDA NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD Not Present O Not Present O Not Present 0 Not Applicable 0 No VOA vials submitted 0 Not Applicable 0 Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Contact and Corrective Action Comments: None Page 32 of41 Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: Energy Laboraties Contact: Garrin Palmer ~2~3~93~S~al~t~C~re~e~k~H~wy--.--------------Ph;4356782221 Casper WY, 82601 gpalmer@energvtuels.com Chain of Custody/Sampling Analysis Request p . t ro)ec s amplers N a me s amplers SigruttuJe 4th Quarter Air 2016 Garrin Palmer I /:J>VA_~ CY~ \..._../ Time SampleiD Date Collected Collected Laboratory Analysis Requested BHV-1 9/27/16-12/27/16 NA U-NAT, TH-230, Ra-226, Pb-210, TH-232 BHV-2 9/27/16-12/27/16 NA U-NAT, TH-230, Aa-226, Pb-210, TH-232 BHV-4 9/27/16-12/27/16 NA U-NAT, TH-230, Aa-226, Pb-210, TH-232 BHV-5 9/27/16-12/27/16 NA U-NAT, TH-230, Ra-226, Pb-210, TH-232 BHV-6 9/27/16-12/27/16 NA U-NAT, TH-230, Ra-226, Pb-210, TH-232 BHV-7 9/27/16-12/27/16 NA U-NAT, TH-230, Ra-226, Pb-210, TH-232 BHV-8 9/27/16-12/27/16 NA U·NAT, TH-230, Ra-226, Pb-210, TH-232 Blanks 9/27/16-12/27/16 NA U-NAT, TH-230, Ra-226, Pb-210, TH-232 Comments: Please send report to Kathy Weinel at kweinel@energytuels.com -----------------'-------·--· ·-. Date/Time l-(s. .. l"1 O;)O Date/Time Page 33 of 41 Energey Fuels Resources-White Mesa Mil Cahbratton Date: 717/2016 First Monitoring Quaner 2015 BHV-1 Period: September 27th, 2016-December 27th, 20lt Calibration Slope & Intercept: m~ I 25008 b~ -0 0206 Updated: 7/30/14 Orifice SIN 8091779 IIH IIH 1111 Ta Tot Po Oil Qf ,QJ iotpl Week Filter Start Slop Slart Stop 'r0!41 Starting Stopping AV!Of'il< Wkly,Avg \YIIb·· A•B· Wkly. Avg 1\<il.flow 'SOl Flo•• 1 s!d flo•• Ill 1'll'o 01'011 w •• L<lodl,. Por«nl # Number Dale Date Time Time l'lloo Manometer Manometer Mi"''IIJOI<! Temp. Tc!np, Pressure l!i<JFM~ Vol•OJC Wolalll w:r W<i""t ~) (1))10) (in H,O) (in H20) (lit. fi,Q) (oC) (J() (mmHg) (OJ'Imuoj (m'lml~l tn'lmlft) (m') w o•lll (IJIJIIU') (% I 9220194 912712016 10/3/2016 76133.49 76277.8 8658.6 4,0 4.0 4.0 16.1 289.2 (>2.23 U l 093 32g} 8087 7 4 3538 4.4394 85 6 0 0106 85 9 2 9220193 10/312016 10/1012016 76277_8 76448..15 10245.0 4.0 4.0 40 115 284.6 62(LJ 1.10 094 33.20 963L7 43557 4,4R48 129.1 00134 101 6 3 9220185 10/10/2016 10/1712016 76448.55 76611 91 9801,6 4.0 4.0 4.0 IS 8 289.0 6198 1.11 0..93 32..93 91406 4.3305 4.5341 203.6 00223 97.2. 4 9220170 10/17/2016 1012412016 76611.91 76780,87 10137 6 4.0 40 40 126 285 7 621.8 1.10 0.94 33 18 9524 s 4 3564 4.5747 218.3 0..0229 100..6 5 9220169 10124/2016 10131/2016 76780.87 76948.24 10042.2 4.0 4.5 4.3 14.3 287 5 6226 114 097 34.10 %963 4.3662 4.4985 132.3 00136 996 6 9220154 10/3112016 111712016 76948.24 77112 78 9872-4 4.0 4.0 4.0 11.2 284.3 621.79 1.10 094 33 2~ 9298 0 4 3754 4Afi34 880 0 0095 979 7 9220146 IIJ7fl.01 () 11114/2016 77112_78 772.8136 10114 8 4.0 4.0 40 9,4 282 6 614_&4 1.09 0.95 3H5 9579.1! 4.32.53 4.4341 108.8 0 0114 1003 8 9220144 ll/141201~ 1ll21/2.016 7728l36 77448 15 [0007.4 4,0 4,0 40 69 280.1 620.77 1,09 0 95 3349 9489 6 4 3461 4.6006 254.5 0.0268 ~ 9 9220136 11/2112016 IU2Ril016 77448.15 77616.42 10096.2 4.0 4.0 40 3.3 276 4 619 50 I 09 095 33 68 9628 2 4 3546 4,4430 88.4 0 0092 100..2 10 9220129 11/28/2016 1215/2016 77616.42 77785.28 101316 4,0 4.0 40 ·12 ...2Z..!L. (,16.96 1.08 096 33 89 97222 4 3554 4 4087 53 3 0 0055 100_5 II 9220114 12/512016 12/1212016 77785,28 77952 87 10055.4 4.0 4.0 40 ·~ 273 9 fll899 I. OR 0.96 33_82 9~29 6 4 3024 43989 965 0 0100 99 8 l2 9220112 J2f12L2D1tl 1211912016 77952_87 78125 61 10364.4 4,0 4.0 4.0 ~ 274 4 618.49 1,08 096 33 Jj 991L6 4...3529 4;.162.6 109,7 QOIIL ~~ 13 9220105 12119/2016 12127/2016 78125.61 78316.49 11452 8 4.0 4,0 40 -1.0 272.J 620 01 I_ OR 09fi 33 96 11013 6 4 3543 4.4138 595 0 0054 113.6 Totals 130980.0 14.24 1234 43~ 71 l24353.5 56 529 5R 157 1627 6 0 1716 Averages 10075,4 4,0 4.0 4.0 7,8 280 9 620 61615 I 10 0 95 33..52 9565 7 4_148 4 474 125.2 0 0132 1000 Comments: Insert weekly-flow check values in yellow columns Bh..,c\)lumn ••h,.ut ._toU)Oiecl <llun columns are calculated avemges from the met sl8tion. _j 1'-.tnltor'tftl*'iiltiiillrii"riiioeoltiiiiiL Page 34 of 41 Energey Fuels Resources-White Mesa Mil Calibration Date: 7/7/2016 F1rst Momtonng Quaner 2014 BHV-2 Period: September 27th, 2016-December 27th, 201 € Calibration Slope & Intercept: m= I 25008 b= -0.0206 Updated: 7/30/14 Orifice SIN: 8091779 1111 1111 ·t.H To To Po •Qo 0. Qo Tot>l Week FilLer Siart Slop Slort Stop l;o,.l SL.arting Slopping Aw•i~$· Wkly.Avg WJ\1) "~' Wkly. Avg A<t FlO": Std flo~ Sid I'Jqw S.d, ,..,. a... "'" Loodqt~ P~cnt # Number Date Dote Time Time l one Monometcr Manomeler MOiJ"f1'<tor Temp. Temp. Pressure (SCflll) Volynu: Wtllfn Wtltlll We{p l Onllnwn (nur~ (in H20) (in H20) tln,ll,O) (OC) (1:)11_ (mmHg) (da'lmlr.) (m~hnln) tO'Imln) •(1\\'1 fa) Ia)_ (mti) (mlll>!:l (%) 1 9220195 9127/2016 10/3/2016 86741 28 86886 28 8700 40 40 40 161 289,2 62230 Ill 093 32 99 8126.3 4 3523 4 4709 118.6 o.ot•6 86.3 -+-9220192 10/3/2016 10/10/2016 86886.28 87057.05 L0/!16.2 40 40 40 115 284.6 620.16 110 094 33.20 9632,8 43472 4.5094 162 2 00168 ~ 3 9220184 10/10/2016 10117/2016 87057.05 87220.56 1}8106 40 40 40 15 8 289.0 fil9 7fi 1,11 093 32.93 9149,0 4 3176 4 6099 292 3 00319 973 4 9220171 10/17/2016 10/24/2016 87220 56 87388 86 10098 40 40 4.0 12 G 285 7 621 79 1.10 0.94 33 18 9487,3 43666 4 6007 2341 0 0241 100 2 5 9220168 10/24/2016 10/31/2016 87388.86 87556 02 10029.6 4.0 45 43 14 3 287,5 622 6 I 14 0 97 34 10 9684 2 43781 4 6033 225 2 0 0233 99 6 9220155 10/31/2016 11/712016 87556.02 87726.01 10199.4 4.0 4.0 40 112 2843 62179 I 10 094 33 26 96060 43633 4.5917 2284 00138 1012 7 9220147 11/7/2016 11114/2016 87726 01 87894.48 ~ 40 40 4.0 94 282 6 624 84 1,09 095 33 45 9573 5 43094 4.4901 180 7 0 0189 1003 8 9220143 11/14/2016 11/2112016 87894 48 88060 64 9969.6 4.0 40 40 6.9 280 I 620 77 I 09 0.95 3349 9453 7 43456 4 6238 278 2 0 0294 989 9 9220135 11/21120 16 11/28/2016 88060.64 88229 73 10145,4 4.0 4.0 40 33 276.4 619 50 1,09 0.95 33 68 9675 2 43473 4 4446 973 0 0101 1006 l'o 9220128 I 1/18/2016 12/5/2016 88229,73 8839U7 10082 4 40 4.0 4.0 -I 2 2719 616.96 1.08 0,% 33 89 %750 4.3501 4.4613 Ill 2 0 0115 1000 II 9220115 12/5/2016 12/12/2016 88397,77 88564 73 10017 6 40 50 4.5 0.8 273 9 61899 1.15 1.01 35 84 101665 43876 4 5557 168 I 0 0165 994 12 9220111 12/12/2016 12/19/2016 88564,73 88737 73 103MU 40 4.0 40 1.3 274.4 618.49 1,08 096 33.77 9926,5 4 3465 4.4980 151.5 0 0153 ~ 13 9220104 12/19/2016 1212712016 88737,73 88928 38 11439 40 40 40 ·I 0 272,1 620.01 1.08 096 33 96 11000_4 4.3500 '-4160 7~ 0 0070 1135 Totals 131226.0 14 30 1.2.40 437.73 1251564 56 562 58886 2324 7 0.2437 Aver_a.ges 10094 3 40 4 I 41 78 280,9 620,61615 1,10 0 95 33 67 9627.4 4_351 4.530 178 8 00187 100 I qmmcnl\: fnsert weekly flow check-values in ycUow columns Bill!) aoiWliP r•l~~ ,(ll..,.kula~ed Green c:ohunns are calc:ulaled overages from lhc met sl.alion, liiiiilllllt~-1 Page 35 of 41 Energey Fuels Resources-White Mesa Mill Calibration Date: 7/7/2016 Ftrst Momtonng,Quarter 20I4 BHV-4 Period: September 27th, 2016-December 27th, 2016 Calibration Slope & Intercept: m~ 125008 b~ -0 0206 Updated: 7/30/ I 4 Orifice SIN: 8091779 "" Ml 611 Ta ,.. Pa Q:o Ql Ql ToW Week Filter Slart StoP, Stan Stop lll>!oJ Starting Slopping A\CfDiiQ' Wkly,Avg Wkft.>\•1-Wldy.Avg Ad. flo~· Sol FloW Sid.""" Sid-1M a-li<t Lqodll8 Pcr«n1 N Number Date Dale Time Time time M:mtnUcle.r Manometer ,MoOOIIId~ Temp ~ ... Press'"" ~~~· Volume w:' Wtf \\leljlll Orut~ Cnoin) (in H1Q) (in H20) l·~ 11,0) ('C) (I() (mmHg) (m'lml~l ,,~·'·"•1 (nl'l (IIIJ.I (mt/d() (% I 9220196 9127/2016 10/3/2016 61925 il 62072 75 8822.4 4.0 4.0 40 16 I 289 2 622,30 1,11 093 32 99 82406 4.367M 44ot&7 80.9 00098 ~ 2 9220191 10/3/2016 10/10/2016 62072 7 62UO 82 10084 2 4.0 4,0 40 115 284 6 620,26 LlO 094 33 20 9480 5 4 3697 44938 124 I 00131 1000 3 9220183 10110/2016 10/17/2016 62240 82 62.,05.68 9891.6 4.0 40 40 15 g 2890 619,76 1.11 0 93 32.93 9224 6 4.3152 4 5095 1943 00211 98 I 4 9220172 10/17/2016 10/H/2016 62405 68 62575.26 10174_8 4.0 40 40 126 285 7 621,79 1.10 0.94 33,18 9559.5 0406 45175 176 9 00185 1009 5 9220167 10/2-1/2016 10/31/1016 62575.26 62741.87 99%.6 40 50 45 143 287 5 622 6 I 17 0?9 35.07 9928.1 ... 3821 4 5225 1404 00141 ?92 6 9220156 10/31/2016 1117/2016 62741.87 62909.92 10083 40 40 4.0 U,l 284 3 621,79 110 0 94 33.26 9496.4 4 3606 4 4202 59,6 0,0063 1000 7 9220148 JJ/7/2016 1111412016 62909.92 63078.61 10121.4 40 40 4.0 94 282 6 624,84 I 09 0 95 33.45 9586.0 4 3059 4 4152 109 3 0,0114 1004 8 9220142 11/14/2016 11121/2016 6307861 63246 38 10066 2 40 40 40 69 280 I 620 77 I 09 095 33.49 9545 3 4 3706 4 5496 1790 00188 99.9 9 9220134 1111:l1201li IJ/28nOI6 63246_38 63414 82 10106.-1 40 40 40 33 276" Gl?.lt> I 09 095 );.GS %38,0 4.3586 4-1257 67.1 O.oolU lOll 10 9220127 11128/2016 12/S/1016 63414 82 63583 59 101.2<1.1 40 40 40 -12 271 9 61696 I 08 096 33,89 9717.0 4 3616 4 4076 46.0 00047 1110,5 II 9220116 12/5/2016 1211212016 63583 59 63749.78 9?71.4 40 40 40 08 273.9 618 99 I 08 096 33 82 9549 2 4 3757 44721 96.4 0,0101 98 9 ""'12 9220110 12/12/2016 12119/2016 63749 ;g 63921.94 IQ329 o 40 40 40 1.3 274.4 618 49 I 08 096 33.77 9878 3 4 3821 44753 93.2 0.0094 102.5 13 9220103 12/19/2016 12/2712016 6392194 fi411l R 11391.6 40 40 40 -1.0 272.1 ll20.0l I 08 096 33,96 10954.8 4.3676 4.4110 41.4 0.0040 113 0 Totals 131165,4 14_27 1237 -13669 124798 J 56Ji5R 5RJlll9 14106 0,1482 Avern.ees 10089 6 40 4 I 40 78 2809 620 61615 1.10 095 J3..59 9599 9 4_358 4467 JOSS 0,011-1 100.1 Commrnt11: Insert weekly flow check vaJues in yellow colunms Uluoqolunm >'I!IICI.IIIt'tlltul~od, G~~=-~~~~~ns ;uo ad~~dAltd-a:\Cfl)p rram lhc mel Sl8Uon QQIIM, Page 36 of41 1Energey Fuels Resources-White Mesa Mil Calibration Date: 717/2016 First Momtonng Quarter 2014 BHV-5 Period: September 27th, 2016-December 27th, 20lf Calibration Slope & Intercept: m~ 1.25008 b~ -0.0206 Updated: 7/30114 Orifice SIN: 8091779 IIH 1m ·li.H Ta To Po q. Ql Ql To !Ill' Week Filter Sian Stop Stan Stop Ta1al Sturting Stopping Awoac Wkly.Avg \Wklt·'"'* Wkly.Avg ..... ~loll SIIIJ FJon 5'14, Flo\\!_ Sid ~e Gnloo Net l"lJdlqJ Pct~:tnl # Number Date Date Time Time n,., Manomclcr Mlli!OJUC:I(r MllllOI!t<t~t Temp. 'l'emp. P~essure ~~ Vbloli1>< w:a w: W<ihl OnJtiWII (mlnf (in H20) (in H,O) (tn,U,OJ ("C) I~) (mmHg) (m'lnltn) (m'lmlll) (m>j ("'II) '(milftn'l (~) I 9220197 912712016 101312016 85450 98 85597.62 8798 4 40 40 40 16 I 2892 622 30 I ll 093 32-99 8218 2 4 35]4 4 4360 82 6 0.0101 87..1 2 9220190 10/3/2016 10/10/2016 85597 62 85766.12 10110 40 40 40 II 5 2846 620..26 I 10 094 33.20 9504 8 4 3738 45187 144.9 00152 1003 3 9220182 10/10/2016 10/17/2016 85766 12 85930.92 9R88 40 40 40 15 8 2890 619 76 Ill 093 32.93 9221.2 4 2864 4 4906 204 2 0,0221 98.1 4 9220173 10/17/2016 10/24/2016 85930 92 86100.46 101724 4 0 40 40 12 6 285 7 621 79 I 10 094 33.18 9557.2 4 3557 4.5718 216 I 0,0226 1009 5 9220166 10/24/2016 10/31/2016 86100.46 86267.29 10009 8 40 40 40 14 3 287 5 622.6 I 10 094 33 10 9380 7 4 3721 4 5002 1281 0.0137 99..1 6 9220157 1013112016 11/7/2016 86267 29 86434.82 10051.8 4.0 40 40 11.2 2843 621 79 I 10 094 33 26 9467 0 4 3932 4 4884 95 2 0 0101 99.7 7 9220149 11/712016 11114/2016 86434 82 86603 5 101208 4.0 4.0 40 94 2826 62484 109 0.95 33 45 9585.5 4 3359 4 4364 1005 0.0105 1004 8 9220141 11/1412016 11121/2016 86603.5 86771.61 10086.6 40 40 4.0 69 280 I 620 77 109 095 3349 9564 7 43794 4.5844 205 0 0,0214 100 I 9 9220133 1112112016 11/28/2016 86771.61 86940.1 10109.4 40 40 40 3.3 276.4 619.50 1.09 095 33 68 9640 8 4 3932 4.4672 74.0 0.0077 1003 10 9220126 11128/2016 12/5/2016 86940 I 87108 81 10122.6 4.0 4.0 4.0 ·I 2 271.9 616.96 1.08 0.96 33 89 9713 5 4 3396 4.3967 571 0 0059 100 4 II 9220117 12/5/2016 12112/2016 87108.81 87274 65 9950 4 4.0 4.0 50 0.8 2739 61899 L21 1.07 37.75 10636.7 4.3893 4.4739 84,6 00080 98,7 12 9220109 12112/2016 12119/2016 87274 65 87447 13 1034K8 40 40 40 1.3 274.4 618.49 1.08 096 33 77 9896 6 4 3878 4.5044 116.6 0.0118 102.7 13 9220102 12/19/2016 12127/2016 87447 13 87636 68 11373 4 5 40 43 -1.0 272.1 620 01 1.11 0.99 34.99 11268 3 4.3333 44004 67.1 00060 112 8 Totals 1311420 14.36 12A5 439.67 ll.'i655.3 56693 5R 269 1576.0 0,1649 Averaees 100878 40 40 4 I 78 2809 620 61615 1.10 0% 33 82 %658 4.361 4_ .. 82 121_2 00127 100 I Comments: Insert weekly flow check vnlues in yellow columns Oloc •~lumn>atoy·orv nl<u!Jtlold Green columns are calcul&ted G\'UIIISC. 'h:m lhe met slation . .............. ·"'~lttlo-~ Page 37 of 41 Energey Fuels Resources-White Mesa Mil Calibration Date: 7/7/2016 First Monitoring Quarter 2014 !BiW-6 Period: September 27th, 2016-December 27th, 201 E Calibration Slope & Intercept: m~ 1.25008 ~ -0.0206 Updated: 7/30/14 Orifice SIN· 8091779 IIH IIH 411 To '1'1 Pa Qll ~ Qo T~t Week Filler Slart Stop Slart Stop To<ot SLarting Stopping ll•mll!' Wkly. Avs. Wl:l)'• "11 Wkly. Avg ~CL Flo-< Sjd. ~1i!jll ~~IL~ll Sid ~ an... l!(<t LDDdln; p • ....,., # Number Date Date Time Time 'li"'• ftdanomclc:r Manometer. MqM'lJl.' Temp IJ'm~p Pressure tS0€1-i) 'vo!lil\1< Wolpl w;r W<l•llt 9·-•(ml~) (!!lo_H,O) (in H20) (ln.H ·) (C) {!:). (mmHs) {oi'IMIJI) (m:finni\) .tnllmlft) (m'j, Ill. l••u \rni!Jnt! (~> 1 9220798 9/27/2016 10/3/2016 1863.7 2010 7 8820 40 40 40 16 I 289 2 622 30 1.11 093 32.99 82384 4.3308 4.4170 86 2 0.0105 87.5 2 9220189 10/3/2016 10/10/2016 2010.7 2178.83 10087_8 4.0 40 4.0 11.5 284 6 ~ 1,10 094 33 20 9483,9 4.3769 44683 91 4 00096 100 I 3 922018t 10/10/2016 10/1712016 217883 2343.64 9888 6 40 40 40 15.8 289.0 619.76 1.11 093 3293 9221.8 4.3366 4.4675 1309 0.0142 98_1 4 9220174 10/17/2016 10/24/2016 2343 64 2513 2 10173 6 40 40 40 12 6 285,7 621.79 1.10 094 33 18 9558 3 4.3594 4.5582 1988 00208 1009 5 9220t58 10/24/2016 10/3112016 2513,2 2679,93 10003 8 40 50 4,5 143 287 5 622 6 117 099 35 07 9935 2 43686 44905 121 9 00123 992 ~ 9220158 10/31/2016 1117/2016 2679 93 2847.85 10075 2 40 40 40 112 2843 621 79 1.10 094 33 26 9489 0 43559 44406 84 7 00089 1000 7 9220150 11/7/2016 11/14/2016 2847 85 3016.55 101.22 40 40 4.0 9.4 282.6 624.84 I 09 095 3345 9586 6 43279 44298 1019 00106 1004 ~ 9220140 11114/2016 11/2112016 3016_55 3184,36 10068 6 40 40 40 69 280.1 620 77 I 09 0.95 3349 95476 43851 46112 226 I 00237 999 r-t-9220132 11/21/2016 11/28/2016 3184_36 3352 8 10106.4 4.0 40 4.0 33 276.4 619 50 I 09 095 33 68 9638 0 43814 ~ 65 5 00068 1003 10 9220125 11/28/2016 12/5/2016 3352,8 3521.56 10125.6 4.0 45 4_3 -1.2 271.9 616.96 I. II 099 34.91 10010.9 4.3493 4.4139 64.6 0.0065 100.5 11 9220118 12/5/2016 12/12/2016 3521 56 3687.79 9973 R 40 4 0 4.0 08 273.9 618.99 1.08 0.96 33.82 ~ 4.3590 ~ 102 I 0.0107 98.9 ~ 9220108 12112/2016 12/19/2016 3687.79 3859.89 10326 4.0 4.0 4.0 13 274 4 618 49 I 08 096 33 77 9874 8 43699 44664 96 5 00098 102 4 ~ 9220101 12/19/2016 12/27/2016 3859.89 4049.78 11393.4 ~ 4.0 4..0 -1.0 272.1 620.01 1.08 ([96 33.96 10956..5 4..3442 4.4143 70 I 0.0064 I 13.0 Totals 131164 8 1430 1239 43771 l250921l 56.645 .5&.086 14407 01507 Avera!les 10089.6 40 4.1 4.1 7.8 280.9 620.61615 1.10 0.95 33.67 9622.5 4.357 4.468 110.8 0,0116 100,1 Cummcnls: Replaced Elapsed LLme md1cator on 7n 112016 Insert weekly now check values in yellow columns. Q1 .. •c:ol"'ll~'"'~~ Green columns are calculated averages from the met station Page 38 of 41 Energey Fuels Resources -Vv'hite Mesa Mil Cailbratwn Date: 7/7/20t 6 Fmt Monitoring Q uarter 2014 BHV-7 Period: September 27th, 2016 -December 27th, 201E Calibration Slope & Intercept: m~ 1.25008 b~ -0.0206 Updated: 7/30/14 Orifice SIN: 8091779 C.H C.H All Ta To Pa 0t Qs, Qo 1'blll Week Filler Stan Stop Stan Stop 1'9<11 Starting Stopping "'~'"a<> Wl<ty Avg W):~ AJ Wl<ty. Avg AI:! f'low' S!d\1'1.)" lil'l-~: Soli! Tn Oo\llo Net Loodoot Pc~t # Number Date Date Time Time Tamo, Manometer Mimomctor l<\1111<11\lGICT Temp Tc~(' Pressure ( PM) vt~";'· w:• w;r WcioJ>I Onslream (min) (in H,O) (in H,O) (l'A.11,0) (oC) . CK (mmH!!) (ftl'hlllo) tm'lnil!l) (n'lnolnl (mM) {mJin(,) ~) I 9220199 9127/2016 J0/3/201G 14123 69 14267.33 86304 40 4.0 4,0 161 289.2 62230 1.11 093 3299 8061 3 43116 43788 67.2 00083 85.6 2 9220188 1013/2016 10110/2016 14267 53 14438 II 10234_8 40 4.0 4.0 11 5 284.6 62026 t.lo 094 33.20 9622 I 4 3537 4 4614 1077 00112 101 5 3 9220180 1011012016 1011712016 14438 II 14602 9833 4 40 4.0 40 15 8 289.0 619 76 1.11 093 32.93 91703 4.3272 4 5187 191 5 00209 97,6 4 9220175 10/1712016 1012412016 14602 14770 64 101184 40 4.0 40 12 6 285.7 621 79 110 094 33 18 9506.5 4.3492 4 5210 171 8 00181 1004 5 9220164 !012412016 1013112016 14770 64 14938 35 10062 6 40 40 40 14 3 287,5 622 6 I 10 094 33 10 9430 I 43432 44507 107 5 00114 99,8 6 9220159 1013112016 1tn12o16 14938 35 15106 95 10116 40 40 40 112 2843 621 79 1.10 094 33 26 9527 4 43436 44274 83 8 00088 100 4 7 9220151 1117/2016 11/1412016 1510695 15275 67 10123.2 40 40 40 94 282,6 62484 109 0.95 3345 9587 8 4 3586 44634 104 8 00109 1004 8 9220139 11114/2016 llf2112016 15275.67 15442 91 10034 4 40 40 40 69 280 I 620 77 109 095 33 49 9515 2 4,3661 4 5644 1983 0 0208 99.5 9 9220131 1112112016 1112812016 1544291 15611.2 10097.4 40 4.0 4,0 3.3 276,4 619,50 109 095 33 68 96294 43718 44457 73 9 0 0077 100 2 10 9220124 11/28/2016 12/512016 15611 2 15780 03 10129.8 40 4.0 4.0 -1.2 271.9 616.96 1.08 0.96 33 89 9720.5 4 3309 43785 47,6 00049 100 5 11 9220119 1215/2016 1211212016 15780.03 15947.12 10025.4 40 40 40 0.8 273.9 61899 1.08 0.96 33.82 9600.9 4.3907 4.4723 81.6 0.0085 99.5 12 9220107 12112/2016 12/19/2016 15947.12 16120.08 10377.6 4.0 ~ 40 ~ 274.4 61849 I 08 096 33.77 9924 2 4 3886 4 5079 1193 0 0120 103 0 13 9220100 1211912016 12/27/2016 16120 08 16310.77 11441.4 4.0 4.0 4.0 ·1.0 2721 620.01 1.08 09~ 33~96 11002.7 0114 4_3784 67.0 0 0061 113.5 Totals 131224 8 14.21 1231 434_71 124298.3 56,j47 579(iQ 14220 0 1496 Avera.ges 10094.2 40 4.0 4.0 7.8 280.9 620 61615 1.09 0.95 33.44 9561.4 4.350 4,459 109.4 0.0115 100 I Comments: lnscrt weekly flow check values in yellow columns Bl110 eolumn >alQC• .,. col<ollalt<l Gruncolunt,ru are «l!tulated averages from the met station lllimJIIIPMli!IICWiil .. Page 39 of 41 Energey Fuels Resources-White Mesa M1l Cahbrat10n Date: 7/T/2016 Ftrst Momtonng Quarter 2014 BHV-8 Period: September 27th, 2016-December 27th, 201E Calibration Stope & Intercept: m~ 1.25008 b~ -0.0206 Updated: 7/30114 Orifice SIN: 8091779 dll dH All Ta To Pa (.t, Qr Qo Tqlal Week Filter Stan Stop SJan Stop Total Stoning Stopping "'""'"'' Wldy Avg ~'y A~ Wldy.Avg ·M I floW1 Std. I'»• Sod tlow ljl r ... an. N91 4Jc>cllns P<~.CCI\1 # Number Date Date Time Time Ti'll• Manometer Manometer lltaoon><J<r Temp. Temp Pressure (SCFI-1) vi~'l!f· w:' W911hl Wcillltl Oruii'O:un 1mln) (in H00) (in H,O) (IJ1.H,0), ("C) (K) (mmHg) (m'/miD) (OI'fl'olrl! tn'imlnl cal tmlll ('mshu') t'~) I 9220200 9/2712016 10(3/2016 501.25 645 6 8661 4,0 35 38 16 L 289 2 622.30 1 07 090 31 ,95 7836. 4 3238 4 3696 458 0 0058 85 9 2 9220187 10/3/2016 10/L0/2016 645,6 81628 10240 8 4,0 4 0 40 1 I 5 284.6 62026 1 10 094 33.20 9627 8 4 3757 4 4289 53 2 0.0055 101 6 3 9220179 10/10/2016 t0117/2016 81628 967,98 9102 4.0 4.0 4.0 158 2890 619 76 Ill 093 32 93 8488 2 4 2938 4 3860 92 2 0.0109 903 4 9220176 10117/20t6 t0/24/20t6 96798 11373 10159 2 4,0 35 38 t2 6 285 7 621 79 t 07 0,91 3214 9246 3 4 3316 44630 131.4 0,0!42 tOO 8 5 9220163 10/24/2016 I0/3J/2016 11373 1304 19 10013 4 4.0 30 3; t4 3 287 5 622 6 1 03 088 30 99 87870 4 3239 43774 l3.l 0.0061 99.3 6 9220160 10/31/2016 11!7/20t6 1304.19 1473 29 10146 4.0 4,0 40 11,2 284 3 621.79 L IO 094 33 26 9lll7 4.3437 43970 53 3 0.0056 100 7 7 9220152 lt/712016 lt/]4/2016 1473.29 1627 69 9264 4.0 4.0 4 0 9.4 2826 624 84 I 09 0.95 33_45 8774.0 43367 4.4014 64 7 0,0074 91,9 8 9220t38 11/14/2016 11/2112016 1627.69 17945 1_0008_6 40 4,0 40 69 280.1 620.77 1.(19 0.95 33.49 9490 7 4.3023 44591 156.8 0.0165 99.3 9 9220130 1 J/21/2016 11/28/2016 1794; 1948 I 9216 40 4,0 4.0 3.3 276.4 61950 1.09 095 33 68 8788 8 4.3813 4_4459 64 6 0,0074 91.4 10 9220123 1 J/28/2016 12/l/2016 1948 I 211692 10129.2 4.0 4.0 4.0 ·I 2 271 9 61696 I 08 0.96 33.89 9719.9 4.3309 43624 315 0,0032 100; II 9220120 1215/2016 12112/2016 2116.92 2284.39 ~ 4 0 6.5 53 08 273 9 6t8 99 1.24 1.10 38.67 11002,9 4 3589 44262 673 00061 99.7 12 9220106 12112/2016 12119/2016 2284.39 2455 5 10266.6 35 4.0 ---2?---1.3 ~ 618 49 1.05 0,93 32,72 9511 0 4,3707 4.4455 74.8 00079 101 9 '""'iJ 9220099 12/19/2016 12/27/2016 2455.5 2616 %30 4.0 4.0 4.0 -10 272 I 620 01 I 08 096 33.96 9260 7 4,3150 434L7 27.7 Oj)OJO 95.5 Totals 126885,0 14.19 1230 434.33 .1.20089.8 56388 57 305 916.8 0.0996 AveraQes 9760.4 4,0 4.0 4.0 7.8 2809 620 6t6t5 t 09 0.95 33.41 92377 4338 4 408 70.5 00077 968 Comments: Tnsert weekly now check vulues in yellow columns !)luc clllumn \'IIIJJ<Oa"'<olcalmd. Green columns an: culcululcd averages from lhe met slatioo. llllillnllller..elaln,.._ialo · -•::::..-"' Page 40 of 41 •:~&imtfl ~:;~i Penod: september 27th, 2016 -w-i "' _ '1f;"'~~.~ t;,\i · , · · 'f?.'U December 27th 2016 '· :'!' ,..,~:!tt:<ff.>i:__,,, Week Fitter Start ·stop Net # Number Date Date 1 9220186 27-Sep-16 03-0ct-16 4.3704 2 9220178 03-0ct-16 10-0ct-16 4.3097 3 9220177 10-0ct-16 17-0ct-16 4.3083 4 9220162 17-0ct-16 24-0ct-16 4.2955 5 9220161 24-0ct-16 31-0ct-16 4.3010 6 9220153 31-0ct-16 07-Nov-16 4.3456 7 9220145 07-Nov-16 14-Nov-16 4.3627 8 9220137 14-Nov-16 21-Nov-16 4.3152 9 9220122 21-Nov-16 28-Nov-16 4.3227 10 9220121 28-Nov-16 05-Dec-16 4.3425 11 9220113 05-Dec-16 12-Dec-'16 4.3336 12 9220098 12-Dec-16 19-Dec-16 4.3539 13 9220090 19-Dec-16 27-Dec-16 4.3323 Totals Page 41 of 41 ATTACHMENT D AIR PARTICULATE LOADING GRAPHS AND SUPPORTING DATA 0 0 0 !=> ..... 0 0 0 ..... 0 0 0 ..... 0 0 0 ..... 0 0 0 ..... 0 0 0 0 1/5/2009 4/5/2009 7/5/2009 10/5/2009 1/5/2010 + 4/5/2010 7/5/2010 OJ :I: < 10/5/2010 I ..... l> + 1/5/2011 -· """' OJ 4/5/2011 (n :I: ,... < 7/5/2011 OJ I ,... N -· + 10/5/2011 0 ::J 1/5/2012 "'C OJ :I: OJ < 4/5/2012 """' I .j::o ,... -· 7/5/2012 n + c: -10/5/2012 OJ OJ ,... :I: tD < 1/5/2013 I l.n r- + 4/5/2013 0 OJ 7/5/2013 c. OJ -:I: ::J < 10/5/2013 OQ I 0'1 -f 1/5/2014 3 OQ OJ 4/5/2014 ......... :I: 3 < 7/5/2014 I w ....... -t 10/5/2014 1/5/2015 OJ :I: < 4/5/2015 I 00 7/5/2015 10/5/2015 1/5/2016 4/5/2016 7/5/2016 10/5/2016 0 0 !=> 1-' b 0 1-' 0 0 1-' 0 0 1-' 0 0 0 0 0 0 0 1/5/2009 4/5/2009 7/5/2009 10/5/2009 1/5/2010 4/5/2010 7/5/2010 10/5/2010 1/5/2011 -:t5F?:. O::J 4/5/2011 j • ~ • < 7/5/2011 I ~ 10/5/2011 ., OJ 1/5/2012 ""'I ,... -· 4/5/2012 n c: -7/5/2012 + OJ ,... 10/5/2012 tD OJ :::c r-< 1/5/2013 0 I 1-' OJ 4/5/2013 a. -· ::::s 7/5/2013 (JQ -10/5/2013 3 1/5/2014 1 I (JQ ......._., . -.... 3 4/5/2014 • ,; .!!A • w -7/5/2014 10/5/2014 1/5/2015 4/5/2015 7/5/2015 10/5/2015 1/5/2016 4/5/2016 7/5/2016 10/5/2016 0 0 !=> ..... 0 0 ..... 0 0 ..... 0 0 ..... 0 0 0 0 0 0 0 1/5/2009 4/5/2009 7/5/2009 10/5/2009 1/5/2010 4/5/2010 7/5/2010 10/5/2010 1/5/2011 -"' 4/5/2011 :I: 7/5/2011 < I N 10/5/2011 ""0 OJ 1/5/2012 ~ -· 4/5/2012 n c - + 7/5/2012 OJ ,... 10/5/2012 tD OJ :I: r-< 1/5/2013 0 I N OJ 4/5/2013 Q. -· ::::J 7/5/2013 CJQ -10/5/2013 3 1/5/2014 CJQ ......._., 4/5/2014 3 w -7/5/2014 10/5/2014 1/5/2015 4/5/2015 7/5/2015 10/5/2015 1/5/2016 4/5/2016 7/5/2016 10/5/2016 0 0 0 p ...... 0 0 0 ...... 0 0 0 ...... 0 0 0 ...... 0 0 0 ...... 0 0 0 0 1/5/2009 4/5/2009 7/5/2009 10/5/2009 1/5/2010 4/5/2010 7/5/2010 10/5/2010 1/5/2011 -c:J 4/5/2011 ::1: .. < 7/5/2011 I .a::. 10/5/2011 ., AJ 1/5/2012 ~ "' -· 4/5/2012 n c -7/5/2012 + AJ "' CJ 10/5/2012 tD :I: ..... < 1/5/2013 0 I .j>. AJ 4/5/2013 Q. -· :::J 7/5/2013 O'Q -10/5/2013 3 1/5/2014 O'Q ........ 4/5/2014 3 w -7/5/2014 10/5/2014 1/5/2015 4/5/2015 7/5/2015 10/5/2015 1/5/2016 4/5/2016 7/5/2016 10/5/2016 0 0 !=> ...... 0 0 ...... 0 0 ...... 0 0 ...... 0 0 0 0 0 0 0 1/5/2009 4/5/2009 7/5/2009 10/5/2009 1/5/2010 4/5/2010 7/5/2010 10/5/2010 1/5/2011 o:J 4/5/2011 :I: 7/5/2011 < I U1 10/5/2011 "C OJ 1/5/2012 ~ -· 4/5/2012 n s:: - + 7/5/2012 OJ ~ 10/5/2012 tD CJ :I: r-< 0 I 1/5/2013 U1 OJ 4/5/2013 Q. -::l 7/5/2013 OQ -10/5/2013 3 1/S/2014 1 ~: I OQ ........ 4/5/2014 3 • 4 ;;~ w • ... ::& • -7/5/2014 10/5/2014 1/5/2015 4/5/2015 7/5/2015 10/5/2015 1/5/2016 4/5/2016 7/5/2016 10/5/2016 !=' 0 0 0 !=' ..... ..... 0 0 ..... 0 0 ..... 0 0 0 0 0 0 0 1/5/2009 4/5/2009 7/5/2009 j ~w 10/5/2009 ~·· 1/5/2010 4/5/2010 7/5/2010 10/5/2010 1/5/2011 4/5/2011 a. :I: 7/5/2011 < I en 10/5/2011 "'tJ AJ 1/5/2012 ""' ,... -· 4/5/2012 n c - + 7/5/2012 10/5/2012 OJ AJ ,... 11) :I: < I 1/5/2013 0'\ r-0 AJ 4/5/2013 Q. -~ 7/5/2013 OQ -10/5/2013 3 1/5/2014 1 4/5/2014 OQ ....... 7/5/2014 3 IN - 10/5/2014 1/5/2015 J __ l!£_ 4/5/2015 j ~ .. =at' .. 7/5/2015 10/5/2015 ~ >l 1/5/2016 . 4/5/2016 7/5/2016 J I ~ 10/5/2016 I I 0 0 0 0 0 !=> I-' I-' I-' I-' 1/5/2015 1/26/2015 2/16/2015 3/9/2015 3/30/2015 4/20/2015 5/11/2015 6/1/2015 6/22/2015 7/13/2015 -o:J :I: 8/3/2015 < I 8/24/2015 ........ 9/14/2015 "'0 OJ ... 10/5/2015 r1' -· n 10/26/2015 c: -f 11/16/2015 OJ r1' tD "' 12/7/2015 :I: r-< 0 I -..J 12/28/2015 OJ Q. 1/18/2016 -· ::::s OQ 2/8/2016 -2/29/2016 3 OQ 3/21/2016 ........ 4/11/2016 3 w -5/2/2016 5/23/2016 6/13/2016 7/4/2016 7/25/2016 8/15/2016 9/5/2016 9/26/2016 10/17/2016 11/7/2016 11/28/2016 0 0 0 0 0 0 0 !=> 0 0 ..... ..... ..... ..... ..... 9/29/2014 10/29/2014 11/29/2014 12/29/2014 I I ~ 1/29/2015 2/28/2015 3/31/2015 4/30/2015 l I ~~oe::-I I o:J I I ::J: 5/31/2015 -l I ~ < I 6/30/2015 -l I ~ I I 00 "'g 7/31/2015 -l I -+. I I QJ ""'' r1' -· 8/31/2015 n r:::: - + 9/30/2015 QJ r1' tD OJ r-:::c 10/31/2015 < 0 I 00 QJ 11/30/2015 c.. -· 12/31/2015 i I ~I I I ::::J OQ -1/31/2016 i I ~ I I I 3 OQ 2/29/2016 i I ~ I ........ 3 3/31/2016 1 I £ I I w - 4/30/2016 5/31/2016 6/30/2016 7/31/2016 8/31/2016 9/30/2016 10/31/2016 11/30/2016 Week # m= 1.25008 b= -0.0206 BHV-2 m= 1.25008 b= -0.0206 Week i Filter # Number 1nno16 BHV-4 m= 1.25008 b= -0.0206 Weeki Filter # Number Energey Fuels Resources -White Mesa Mill Calibration Date: 7n/2016 First Monitoring Quarter 2014 BHV-5 Period: June 27th, 2016-, September 27th, 2016 Calibration Slope & Intercept: m= 1.25008 b= -0.0206 Updated: 7/30/14 Orifice SIN: 8091779 1 ~~-.~ 6H 6H ·: \All'. Tn ~ .. ·1~ •; Pa ,., •. _ 'El'c ~~ /.;.~ ::·~\.' 11 ----1:-~1 \' . -_-' ~-I ·~· ·J--~-· • ~ ·: Week Starting Jf • ... WJ4y. Avg. ~ Wldy. JI:Vg. ·"*"~' '1ili ~.' • ....... \···:1· :·~r· ·~ Filter Start Stop Start Stop Stoppmg ,i..~~ . " __ ,I ::_ .. ~ ~-'· ·. if..:F.~·l:~I ~-. ~1 ~v.·:, ·-............. -~ I # Number Date Date Time Time Manometer Manometer T'lf)'lp. .:• ·I .~sur~ I~ .. ; ...• ~ ... ~. ~~ Iii l~iJ . ~\1.. ·i ~J Jr@DS'; (in. H20) (in. H20) ("C> ':m • (rrunlf~ 'l..~::. Jfliit(, ··~til·"" . ..... :~. ---·' 'I~' ' I 9221201 6/27/2016 7/5/2016 83244.22 83441.98 11865.6 4.0 4.0 4.0 22.6 295.7 621.79 1.12 0.92 32.60 10954.3 4.3033 4.4582 154.9 0.0141 117.7 2 9219794 7/5/2016 7111/2016 83441.98 83579.28 8238 4.0 4.0 4.0 25.7 298.9 619.25 1.13 0.92 32.36 7548.9 4.3841 4.5075 123.4 0.0163 81.7 3 9219786 711112016 7118/2016 83579.28 83750.02 10244.4 4.0 3.5 3.8 25.7 298.8 619.76 1.09 0.89 31.37 9098.6 4.3491 4.5537 204.6 0.0225 101.6 4 9219777 7118/2016 7/25/2016 83750.02 83914.64 9877.2 4.0 4.0 4.0 25.4 298.6 622.55 1.12 0.92 32.47 9080.5 4.3966 4.5668 170.2 0.0187 98.0 5 9219770 7/25/2016 8/1/2016 83914.64 84082.64 10080 4.0 3.0 3.5 27 .0 300.2 620.3 !.06 0.86 30.26 8637.3 4.3452 4.5463 20!.1 0.0233 100.0 6 9219761 8/1/2016 8/8/2016 84082.64 84250.5 10071.6 4.0 4.0 4.0 22.1 295.3 620.77 1.12 0.92 32.60 9297.7 4.3423 4.4733 131.0 0.0141 99.9 7 9219754 8/8/2016 8115/2016 84250.5 84419.32 10129.2 4.0 4.0 4.0 23.6 296.8 620.77 1.12 0.92 32.52 9326.7 4.3816 4.6121 230.5 0.0247 100.5 8 9219745 8/15/2016 8/2212016 84419.32 84588.12 10128 4.0 4.0 4.0 22.6 295.7 620.77 1.12 0.92 32.58 9342.4 4.3431 4.5713 228.2 0.0244 100.5 9 9219738 8/2212016 8/29/2016 84588.12 84757.17 10143 4.0 4.0 4.0 17.7 290.8 621.79 1.11 0.93 32.88 9444.4 4.3460 4.4406 94.6 0.0100 100.6 10 9219729 8/29/2016 9/6/2016 84757.17 84947.95 11446.8 4.0 4.0 4.0 21.0 294.1 620.01 1.12 0.92 32.65 10581.4 4.4016 4.5798 178.2 0.0168 113.6 11 9219722 9/6/2016 9/1212016 84947.95 85092.92 8698.2 4.0 4.0 5.0 21.0 294.2 623.31 1.25 1.03 36.54 8999.1 4.3588 4.5381 179.3 0.0199 86.3 12 9219713 911212016 9/19/2016 85092.92 85258.85 9955.8 4.0 4.0 4.0 17.3 290.4 620.01 1.11 0.93 32.86 9262.5 4.3462 4.5669 220.7 0.0238 98.8 13 9219706 9/19/2016 9/27/2016 85258.85 85450.98 11527.8 4.0 4.0 4.0 15.6 288,8 621.53 1.11 0.93 32.99 10769.8 4.3668 4.5649 198.1 0.0184 114.4 -. Totals 132405.6 14.58 12.03 424.66 122343.7 56.665 58.980 2314.8 0.2472 Averages 10185,0 4.0 3.9 4.0 22.1 295.3 620.96692 1.12 0.93 32.67 9411.1 4.359 4.537 178.1 0.0190 101.0 Comments: Insert weekly flow check values in yellow columns. . . . -· ' .... ~ ~ ::-·_.: .. .:.....:·"--'"--~ Green cohtmns•nre.cnleulaled ·averages· from the met stlllion. I . .. -~"'--.. . ... · .. --....,..,.. -----; BHV-6 m= 1.25008 b= -0.0206 Week I Filter # Number BHV-7 m= 1.25008 b= -0.0206 Week I Filter # Number Energey Fuels Resources -White Mesa Mill Calibration Date: 7nt2016 First Monitoring Quarter 2014 BHV-8 Period: June 27th, 2016-, September 27th, 2016 Calibration Slope & Intercept: m= 1.25008 b= -0.0206 Updated: 7/30/14 Orifice SIN: 8091779 ~H ~ i-:-.a~ . Ta . :tli. .. P-n ··~I ""•Qjl.:.. . QS 'I ~ ·TI:iJiil ~:,) ,,. -:: • I , 4 • 4 I • I;;; ~ Week Filter Start Stop Start Stop .!~.:· Starting Stopping it.~ Wkly.Mt. ~~14 Wkly.AvgJ ~~ I~ I ~~I r ~·. • • ~ ..• ,:1 ~~-, ~ I·.. .. .. ~-1 ···~~ 1-. . I .·--~ # Number Date Date Time Time J!).j Manometer Manometer Temp. ... ~-Pressure ~~ I' • .. :i :r·. ~ -~ ~ : . ., ~ . ~·~ .. !",,,.,.:.._-._•, '":;T~I ··~~ l~ (in. H20) (in. H20) .. riD;~, ( .. C) (riiinflg) ·~ ~~~ l..._t~..._-_1 -!!:.~1 ·' . . ' .... ~-. -··~-· -~ I 9221204 6127/2016 7/5/2016 12380.12 1'2571.9 I 1866.8 4.0 3.5 3.8 22.6 295.7 621.79 1.08 0.89 31.58 10612.7 4.2785 4.4275 149.0 0.0140 117.7 2 9219791 7/5/2016 711 112016 12577.9 12716.77 8332.2 4.0 4.5 4.3 25.7 298.9 619.25 1.16 0.94 33.34 7866.7 4.3587 4.4547 96.0 0.0122 82.7 3 9219783 7/1 1/2016 7/18/2016 12716.77 12886.22 10167 4.0 4.0 4.0 25.7 298.8 619.76 1.13 0.92 32.38 9321.5 4.3561 4.5226 166.5 0.0179 100.9 4 9219780 7/18/2016 7/25/2016 12886.22 13052.08 9')51.6 4.0 4.0 4.0 25.4 298.6 622.55 1.12 0.92 32.47 9148.9 4.3823 4.5099 127.6 0.0139 98.7 5 9219767 7/25/2016 8/1/2016 13052.08 13221.11 10141.8 4.0 4.0 4.0 27.0 300.2 620.3 1.13 0.92 32.32 9281.0 4.3794 4.5439 164.5 0.0177 100.6 6 9219764 8/1/2016 8/8/2016 13221.11 13388.04 10015.8 4.0 4.0 4.0 22.1 295.3 620.77 1.12 0.92 32.60 9246.2 4.3305 4.4129 82.4 0.0089 99.4 7 9219751 8/8/2016 8/15/2016 13388.04 13556.81 10126.2 4.0 4.0 4.0 23.6 296.8 620.77 1.12 0.92 32.52 9324.0 4.3890 4.5251 136.1 0.0146 100.5 8 9219748 8/15/2016 8/2212016 13556.81 13724.48 10060.2 4.0 4.0 4.0 22.6 295.7 620.77 1.12 0.92 32.58 9279.9 4.3853 4.5399 154.6 0.0167 99.8 9 9219735 8122/2016 8/29/2016 13724.48 13893.49 10140.6 4.0 4.0 4.0 17.7 290.8 621.79 1.11 0.93 32.88 9442.2 4.2900 4.3740 84.0 0.0089 100.6 10 9219732 8/29/2016 9/6/2016 13893.49 14083.49 11400 4.0 4.0 4.0 21.0 294.1 620.01 1.12 0.92 32.65 10538.2 4.3534 4.4715 118.1 0.0112 I 13.1 11 9219719 9/6/2016 9/1212016 0 141.54 8492.4 4.0 6.0 5.0 21.0 294.2 623.31 1.25 1.03 36.54 8786.2 4.4033 4.5917 188.4 0.0214 84.3 12 9219716 9/1212016 9/19/2016 141.54 309.12 10054.8 4.0 4.0 4.0 17.3 290.4 620.01 1.11 0.93 32.86 9354.6 4.3765 4.5113 134.8 0.0144 99.8 13 9219703 9/19/2016 9/27/2016 309.12 501.25 I 1527.8 4.0 4.0 4.0 15.6 288.8 621.53 1.11 0.93 32.99 10769.8 4.3806 4.5033 122.7 0.0114 1 14.4 Totals 132277.2 14.68 12.1 I 427.69 122971.7 56.664 58.388 1724.7 0.1833 Averages 10175.2 4.0 4.2 4.1 22.1 295.3 620.96692 1.13 0.93 32.90 9459.4 4.359 4.491 132.7 0.0141 100.9 Comm•niS: Insert weeldy flow check values in yellow columns. L I :~'"·· .. -.. :~·........ ·-· ~ ~ col.umns nre.calculated a'"""&"$ from !he met station.. : . -. . . . . lllliiL -; ---- Energey Fuels Resources -White Mesa Mill Calibration Date: 7nt2016 First Monitoring Quarter 2015 ]~HV-~ Period: September 27th, 2016-December 27th, 2016 Calibration Slope & Intercept: m= 1.25008 b= -0.0206 Updated: 7/30114 Orifice SIN: 8091779 . ~ .. Ml Ml : :Jdf:. • T"ll • .:.tli • Pa i. ~~·r ~(a-ll :... ~~..:-;11 ., .. ,..,,I : 'i I ._-• 1. • ... -·j J , __ . ·- Week Filter Start Stop Start Stop ~--Starting Stopping '.,.~ Wldy.Aovg. ~~ Wld~,A~g. ···~I -~ ·~---·-~·-·1 :i"'~~-_:j ~ ~-I .-:-~ I ':,.c-;·~--_.J ~;a~~· r ~-·---::1 I·~ ~ti.e~ lj-r ;..--·· .,~ ' ·~ .--~_.J # Number Date Date Time Time {,z-. Manometer Manometer Temp. Pressure -~~ ~~1 ~~mrt~ ·@.l~l.i. rCi :~··-\ ·~- .I "' ·~--1)~ ;·~---(in. H20) (in. H20) {nunHg) :.--'-~~ l. '• -~ ·-. -·~: I ,. • -'!"' ! '~. I 9220194 9/27/2016 10/3/2016 76133.49 76277.8 8658.6 4.0 4.0 4.0 16.1 289.2 622.3 ]_]] 0.93 32.99 8087.7 4.3538 4.4394 85.6 0.0106 85.9 2 9220193 10/3/2016 10/10/2016 76277.8 76448.55 10245.0 4.0 4.0 4.0 11.5 284.6 620.3 1.10 0.94 33.20 9631.7 4.3557 4.4848 129.1 0.0134 101.6 3 9220185 10/10/2016 10/17/2016 76448.55 76611.91 9801.6 4.0 4.0 4.0 15.8 289.0 619.8 1.11 0.93 32.93 9140.6 4.3305 4.5341 203.6 0.0223 97.2 4 9220170 10/17/2016 10/24/2016 76611.91 76780.87 10137.6 4.0 4.0 4.0 12.6 285.7 621.8 1.10 0.94 33.18 9524.5 4.3564 4.5747 218.3 0.0229 100.6 5 9220169 10/24/2016 10/31/2016 76780.87 76948.24 10042.2 4.0 4.5 4.3 14.3 287.5 622.6 l.l4 0.97 34.10 9696.3 4.3662 4.4985 132.3 0.0136 99.6 6 9220154 10/31/2016 1117/2016 76948.24 77112.78 9872.4 4.0 4.0 4.0 11.2 284.3 621.79 1.10 0.94 33.26 9298.0 4.3754 4.4634 88.0 0.0095 97.9 7 9220146 1117/2016 11114/2016 77112.78 77281.36 10114.8 4.0 4.0 4.0 9.4 282.6 624.84 1.09 0.95 33.45 9579.8 4.3253 4.4341 108.8 0.0114 100.3 8 9220144 11/14/2016 11/21/2016 77281.36 77448.15 10007.4 4.0 4.0 4.0 6.9 280.1 620.77 1.09 0.95 33.49 9489.6 4.3461 4.6006 254.5 0.0268 99.3 9 9220136 11/21/2016 11/28/2016 77448.15 77616.42 10096.2 4.0 4.0 4.0 3.3 276.4 619.50 1.09 0.95 33.68 9628.2 4.3546 4.4430 88.4 0.0092 100.2 10 9220129 11/28/2016 12/5/2016 77616.42 77785.28 10131.6 4.0 4.0 4.0 -1.2 271.9 616.96 1.08 0.96 33.89 9722.2 4.3554 4.4087 53.3 0.0055 100.5 11 9220114 12/5/2016 12/12/2016 77785.28 77952.87 10055.4 4.0 4.0 4.0 0.8 273.9 618.99 1.08 0.96 33.82 9629.6 4.3024 4.3989 96.5 0.0100 99.8 12 9220112 12/12/2016 12/19/2016 77952.87 78125.61 10364.4 4.0 4.0 4.0 1.3 274.4 618.49 1.08 0.96 33.77 9911.6 4.3529 4.4626 109.7 0.0111 102.8 13 9220105 12/19/2016 12/27/2016 78125.61 78316.49 11452.8 4.0 4.0 4.0 -1.0 272.1 620.01 1.08 0.96 33.96 I 1013.6 4.3543 4.4138 59.5 0.0054 113.6 •. Totals 130980.0 --~ ---~ . -~ 14.24 12.34 435.71 124353.5 56.529 58.157 1627.6 0.1716 Averages 10075.4 4.0 4.0 4.0 7.8 280.9 620.61615 1.10 0.95 33.52 9565.7 4.348 4.474 125.2 0.0132 100.0 Comments: Insert weekly flow check values in yellow columns. ' ~~-:__ __ ~ _ __;____:,__-:.. . :..: ...:1 Green columns ru-e C3lculated awrnges rromlhe Dlclt Station. I •• "'""'' ...... <. ... ... ' ' .-,.....,... ••. ------., - Energey Fuefs Resources -White Mesa Mill ~Calibration Date: 7ni2016 b= -0.0206 1 First Momtoring Quarter 2014 BHV-2 Period: September 27th, 2016-December 27th, 2016 Calibration Slope & Intercept: m= 1.25008 Updated: 7/30/14 - t.H t.H Week I Filter I Stan I Stop I Stan I Stop I ;1lii8J: I Startinc Stopping # Number Date Date Time Time ·-·· I Manome:er Manometer (in. H20) (in. H20) I 9220195 9/27/2016 10/3/2016 86741.28 86886.28 8700 4.0 4.0 4.0 16.1 2 9220192 10/3/2016 10/10/2016 86886.28 87057.05 10246.2 4.0 4.0 4.0 11.5 284.6 620.26 1.10 0.94 33.20 9632.8 4.3472 4.5094 162.2 0.0168 101.6 3 9220184 10/10/2016 10/17/2016 87057.05 87220.56 9810.6 4.0 4.0 4.0 15.8 289.0 619.76 1.11 0.93 32.93 9149.0 4.3176 4.6099 292.3 0.0319 97.3 4 9220171 10/17/2016 10/24/2016 87220.56 87388.86 10098 4.0 4.0 4.0 12.6 285.7 621.79 1.10 0.94 33.18 9487.3 4.3666 4.6007 234.1 0.0247 100.2 5 9220168 10/2412016 10/3112016 87388.86 87556.02 10029.6 4.0 4.5 4.3 14.3 287.5 622.6 1.14 0.97 34.10 9684.2 4.3781 4.6033 225.2 0.0233 99.5 6 9220155 10/31/2016 11/7/2016 87556.02 87726.01 10199.4 4.0 4.0 4.0 11.2 284.3 621.79 1.10 0.94 33.26 9606.0 4.3633 4.5917 228.4 0.0238 101.2 7 9220147 11/7/2016 11/1412016 87726.01 87894.48 10108.2 4.0 4.0 4.0 9.4 282.6 624.84 1.09 0.95 3345 9573.5 4.3094 4.4901 180.7 0.0189 100.3 8 9220143 1111412016 11/2112016 87894.48 88060.64 9969.6 4.0 4.0 4.0 6.9 280.1 620.77 1.09 0.95 33.49 9453.7 4.3456 4.6238 278.2 0.0294 98.9 9 9220135 11/2112016 11/28/2016 88060.64 88229.73 10145.4 4.0 4.0 4.0 3.3 276.4 619.50 1.09 0.95 33.68 9675.2 4.3473 4.4446 97.3 0.0101 100.6 10 9220128 11/28/2016 1215/2016 88229.73 88397.77 10082.4 4.0 4.0 4.0 -1.2 271.9 616.96 1.08 0.96 33.89 9675.0 4.3501 4.4613 111.2 0.0115 100.0 II 9220115 1215/2016 1211212016 88397.77 88564.73 10017.6 4.0 5.0 4.5 0.8 273.9 618.99 1.15 1.01 35.84 10166.5 4.3876 4.5557 168.1 0.0165 99.4 12 9220111 1211212016 12119/2016 88564.73 88737.73 10380 4.0 4.0 4.0 1.3 274.4 618.49 1.08 0.96 33.77 9926.5 4.3465 4.4980 151.5 0.0153 103.0 13 9220104 12/19/2016 12127/2016 88737.73 88928.38 11439 4.0 4.0 4.0 -1.0 272.1 620.01 1.08 0.96 33.96 11000.4 4.3500 4.4269 76.9 0.0070 113.5 Totals 131226.0 14.30 12.40 437.73 125156.4 56.562 58.886 2324.7 0.2437 Averages 10094.3 4.0 4.1 4.1 7.8 280.9 620.61615 1.10 0.95 33.67 9627.4 4.351 4.530 178.8 o.o187 I 100.1 Energey Fuels Resources • White Mesa Mill Calibration Date: ?n/2016 First Monttoring Quarter 20 I 4: BHV-4 Period: September 27th, 2016-December 27th, 2016 Calibration Slope & Intercept: m= 1.25008 b= -0.0206 Updated: 7/30/14i Orifice SIN: 8091779 I I'.H t.H ·~ .rfli :, . 'l'ii l'a ~ • ,Q( ·,. ·4f: . :· 'f@,.: i' i ··~i: '•} . ~~~; Week Filter Start Stop Start Stop 'ror.J. Starting Stopping A~ Wl;ly. Avg. ~A.~ Wkly.A"ll. ·ACt Raw. ·~~--~ '&It • ')~' I .li®. ;~~-~: ·--~~-.. v~:. 1,.~ ,~1 ·-~-. I~ # Number Date Date Time Time Mo.nometer Mnnometd TemJ!. P~u."' ·c.r~-' ( ... ; ' ' ::~:, 8L (in. H,O) (in.H,O) (•CJ _;_' ·~t . (mmHg) (~-~, -·""""-"~ 'Cft:'~. -~-.1 ~ L..l§~u .. ~- I 9220196 912712016 10/3/2016 61925.71 62072.75 8822.4 4.0 4.0 4.0 16.1 289.2 622.30 1.11 0.93 31.99 8240.6 4.3678 4.4487 80.9 0.0098 87.5 2 9220191 10/3/2016 10/10/2016 62072..75 62240.82 IOOS4.2 4.0 4.0 4.0 11.5 284.6 620.26 1.10 0.94 33.20 9480.5 4.3697 4.4938 124.1 0.0131 100.0 3 9220183 10/10/2016 10/17/2016 62240.82 62405.68 9891.6 4.0 4.0 4.0 15.8 289.0 619.76 1.11 0.93 32.93 9224.6 4.3152 4.5095 194.3 0.0211 98.1 4 9220172 10117/2016 10/2412016 62405.68 62575.26 10174.8 4.0 4.0 4.0 12.6 285.7 621.79 1.10 0.94 33.18 9559.5 4.3406 4.5175 176.9 0.0185 100.9 5 9220167 10/24/2016 10/3112016 62575.26 62741.87 999M 4.0 5.0 4.5 14.3 287.5 622.6 1.17 0.99 35.07 9928.1 4.3821 4.5225 140.4 0.0141 99.2 6 9220156 10/31/2016 IIn/2016 62741.87 62909.92 10083 4.0 4.0 4.0 11.2 284.3 621.79 1.10 0.94 33.26 9496.4 4.3606 4.4202 59.6 0.0063 100.0 7 9220148 11n/20I6 11/14/2016 62909.92 63078.61 10121.4 4.0 4.0 4.0 9.4 282.6 624.84 1.09 0.95 33.45 9586.0 4.3059 4.4152 109.3 0.0114 100.4 8 9220142 11/14/2016 11/21/2016 63078.61 63246.38 10066.2 4.0 4.0 4.0 6.9 280,1 620.77 1.09 0.95 33.49 9545.3 4.3706 4.5496 179.0 0.0188 99.9 9 9220134 11/21/2016 ll/28/2016 63246.38 63414.82 10106.4 4.0 4.0 4.0 3.3 276.4 619.50 1.09 0.95 33.68 9638.0 4.3586 4.4257 67.1 0.0070 100.3 10 9220127 11/28/2016 12/5/2016 63414.82 63583.59 10126.2 4.0 4.0 4.0 -1.2 271.9 616.96 1.08 0.96 33.89 9717.0 4.3616 4.4076 46.0 0.0047 100.5 II 9220116 12/5/2016 12/12/2016 63583.59 63749.78 9971.4 4.0 4.0 4.0 0.8 273.9 618.99 1.08 0.96 33.82 9549.2 4.3757 4.4721 96.4 0.0101 98.9 12 9220110 12/12/2016 12/19/2016 63749.78 63921.94 10329.6 4.0 4.0 4.0 1.3 274.4 618.49 1.08 0.96 33.77 9878.3 4.3821 4.4753 93.2 0.0094 102.5 13 9220103 12/19/2016 12/27/2016 63921.94 64111.8 11391.6 4.0 4.0 4.0 -1.0 272.1 620.01 LOS 0.96 33.96 10954.8 4.3676 4.4110 43.4 0.0040 113.0 -Totals 131165.4 14.27 12.37 436.69 124798.3 56.658 58.069 1410.6 0.1482 -Avcmges 10089.6 4.0 4.1 4.0 7.8 280.9 620.61615 1.10 0.95 33,59 9599.9 4.358 4.467 108.5 0.0114 100.1 CoTill11Cnts: lnsen weekly flow check values in }'ellow columns. ,_:.._.. .. ;:~: ': : '. Gn:eo columns,m~culatcd·:~verugesfrom•the met station. ~ ~.-..... ·. _..,... .... ---, I ---Energey Fuels Resources -White Mesa Mill Calibration Date: 7n/2016 First Monitoring Quarter 2014 I ~HV-~ Period: September 27th, 2016-December 27th, 2016 Calibration Slope & Intercept: m= 1.25008 b= -0.0206 Updated: 7/30/14 --Orifice SIN: 8091779 till ll.H iAlf I Ta . -1¥ !?,a .. l(l\, •.Qii< I ~~ . ·:TqtjJ :-~' .... !1 ' • I ., -... ·.. -1 Week Filter Start Stop Start Stop ·T0151 · Starting Stopping ft~:· Wkly.·Avg. ,Wfcijo,:"iiii Wkly.AVg. ~~-;Slit•; . : Stdi .. : ·t(ii.. '•I ~. ~- # Date Date Time Time 1'ime Tel)lp. rr..,. .. 1 . ,._. 'I~):· ..YOlmliO II~ I ~ ,~: :7: Number Manometer Manometer Pressure :irtt~: Tutihn'· ~ (in. H20) (in. H20) ,(la.·ii'}O), . (~ ·..m ' {mmllg) ~~ -~-· -'~1 .' IIJ.. w.t_;, ;~.ilt-1 d......lllil.•.c l 1 9220197 9/27/2016 10/3/2016 85450.98 85597.62 8798.4 4.0 4.0 4.0 16.1 289.2 622.30 1.11 0.93 32.99 8218.2 4.3534 4.4360 82.6 0.0101 87.3 2 9220190 10/3/2016 10110/2016 85597.62 85766.12 10110 4.0 4.0 4.0 11.5 284.6 620.26 1.10 0.94 33.20 9504.8 4.3738 4.5187 144.9 0.0152 100.3 3 9220182 10110/2016 10/17/2016 85766.12 85930.92 9888 4.0 4.0 4.0 15.8 289.0 619.76 1.11 0.93 32.93 9221.2 4.2864 4.4906 204.2 0.0221 98.1 4 9220173 10117/2016 10/24/2016 85930.92 86100.46 10172.4 4.0 4.0 4.0 12.6 285.7 621.79 1.10 0.94 33.18 9557.2 4.3557 4.5718 216.1 0.0226 100.9 5 9220166 10/24/2016 10/3112016 86100.46 86267.29 10009.8 4.0 4.0 4.0 14.3 287.5 622.6 1.10 0.94 33.10 9380.7 4.3721 4.5002 128.1 0.0137 99.3 6 9220157 10/31/2016 11nt2016 86267.29 86434.82 10051.8 4.0 4.0 4.0 11.2 284.3 621.79 1.10 0.94 33.26 9467.0 4.3932 4.4884 95.2 0.0101 99.7 7 9220149 lln/2016 ll/14/2016 86434.82 86603.5 10120.8 4.0 4.0 4.0 9.4 282.6 624.84 1.09 0.95 33.45 9585.5 4.3359 4.4364 100.5 O.Dl05 100.4 8 9220141 11/14/2016 11/2112016 86603.5 86771.61 10086.6 4.0 4.0 4.0 6.9 280.1 620.77 1.09 0.95 33.49 9564.7 4.3794 4.5844 205.0 0.0214 100.1 9 9220133 11/2112016 11128/2016 86771.61 86940.1 10109.4 4.0 4.0 4.0 3.3 276.4 619.50 1.09 0.95 33.68 9640.8 4.3932 4.4672 74.0 0.0077 100.3 10 9220126 11/28/2016 12/5/2016 86940.1 87108.81 10122.6 4.0 4.0 4.0 -1.2 271.9 616.96 1.08 0.96 33.89 9713.5 4.3396 4.3967 57.1 0.0059 100.4 II 9220117 12/5/2016 12/12/2016 87108.81 87274.65 9950.4 4.0 4.0 5.0 0.8 273.9 618.99 1.21 1.07 37.75 10636.7 4.3893 4.4739 84.6 0.0080 98.7 12 9220109 12/12/2016 12/19/2016 87274.65 87447.13 10348.8 4.0 4.0 4.0 1.3 274.4 618.49 1.08 0.96 33.77 9896.6 4.3878 4.5044 L 16.6 0.0118 102.7 13 9220102 12119/2016 12/27/2016 87447.13 87636.68 11373 4.5 4.0 4,3 -1.0 272.1 620.01 1.11 0.99 34.99 11268.3 4.3333 4.4004 67.1 0.0060 112.8 Totals 131142.0 -14.36 12.45 439.67 125655.3 56.693 58.269 1576.0 0.1649 . ~ Averages 10087.8 4.0 4.0 4.1 7.8 280.9 620.61615 1.10 0.96 33.82 9665.8 4.361 4.482 121.2 0.0127 100.1 Comments: Insert weekly flow check values in yellow columns . .. .. . . ..... , .. .. •. - . ' -=-I Cr.ee>l columnsarecalcu1a1Cd o.vemges7ro~·t.;.;met suui~~-' I ~iiii;....w.-·.;;.a,...:o;,; .. a., ... :..Mr......, "-1 Energey Fuels Resources -White Mesa Mill Calibration Date: 717/2016 First Monitoring Quarter 2014 BHV-6 Period: September 27th, 2016-December 27th, 2016 Calibration Slope & Intercept: m= 1.25008 b= -0.0206 Updated: 7/30114 Orifice SIN: 8091779 L'.H L'.H ·• ~ ·Ta;. Pa . -,"Qt. :.~.; \~· -l'~. ' -.. _~ f .. i .. - Week Filter Start Stop Start Stop Toilil. Starting Stopping ,A~· Wldy.Avg. ~~·~ Wkly.A\rg. :~~ '-~ ·~~ ' ;'$If. . ·~~-,!· ~·' -~; ~~:: {. :.-.:~_-•, ' ( .~) # Number Date Date Time Time -t~ Manometer Manometer I~ Temp. :TCI!.IJ', Pressure ~(ct(liiiiil>: ~ .. , ·~=~ Yolimle • :~· . I :t_~ey" ODin) C"C> ,00_ ·(biy~. : .(Jil"j · '!iiii:' ~ ~~ I ~ (in. H20) (in. H20) ·(Ia:; ' Inunligl ". I 9220798 9/27/2016 10/3/2016 1863.7 2010.7 8820 4.0 4.0 4.0 16.1 289.2 622.30 1.11 0.93 32.99 8238.4 4.3308 4.4170 86.2 0.0105 87.5 I 2 9220189 10/3/2016 10/10/2016 2010.7 2178.83 10087.8 4.0 4.0 4.0 11.5 284.6 620.26 1.10 0.94 33.20 9483.9 4.3769 4.4683 91.4 0.0096 100.1 3 9220181 10/10/2016 10117/2016 2178.83 2343.64 9888.6 4.0 4.0 4.0 15.8 289.0 619.76 1.11 0.93 32.93 9221.8 4.3366 4.4675 130.9 0.0142 98.1 I 4 9220174 10/1712016 10/24/2016 2343.64 2513.2 10173.6 4,0 4.0 4.0 12.6 285.7 621.79 1.10 0.94 33.18 9558.3 4.3594 4.5582 198,8 0.0208 100.9 5 9220158 10/24/2016 10/3112016 2513.2 2679.93 10003.8 4.0 5.0 4.5 14.3 287.5 622.6 1.17 0.99 35.07 9935.2 4.3686 4.4905 121.9 0.0123 99.2 6 9220158 10/31/2016 1117/2016 2679.93 2847.85 10075.2 4.0 4.0 4.0 11.2 284.3 621.79 1.10 0.94 33.26 9489.0 4.3559 4,4406 84.7 0.0089 100.0 7 9220150 1117/2016 11/14/2016 2847.85 3016.55 10122 4.0 4.0 4.0 9.4 282.6 624.84 1.09 0.95 33.45 9586.6 4.3279 4.4298 101.9 0.0106 100.4 8 9220140 11114/2016 11121/2016 3016.55 3184.36 10068.6 4.0 4.0 4.0 6.9 280.1 620.77 1.09 0.95 33.49 9547.6 4.3851 4.6112 226.1 0.0237 99.9 9 9220132 11/21/2016 11128/2016 3184.36 3352.8 10106.4 4.0 4.0 4.0 3.3 276.4 619.50 1.09 0.95 33.68 9638.0 4.3814 4.4469 65.5 0.0068 100.3 10 9220125 11128/2016 12/5/2016 3352.8 3521.56 10125.6 4.0 4.5 4.3 -1.2 271.9 616.96 1.11 0.99 34.91 10010.9 4.3493 4.4139 64.6 0.0065 100.5 11 9220118 12/5/2016 12112/2016 3521.56 3687.79 9973.8 4.0 4.0 4.0 0.8 273.9 618.99 1.08 0.96 33.82 9551.5 4.3590 4.4611 102.1 0.0107 98.9 12 9220108 12/12/2016 12/19/2016 3687.79 3859.89 10326 4.0 4.0 4.0 1.3 274.4 618.49 1.08 0.96 33.77 9874.8 4.3699 4.4664 96.5 0.0098 102.4 13 9220101 12/19/2016 12/27/2016 3859.89 4049.78 11393.4 4.0 4.0 4.0 -1.0 272.1 620.01 1.08 0.96 33.96 10956.5 4.3442 4.4143 70.1 0.0064 113.0 - Totals 131164.8 -.. 14.30 12.39 437.71 125092.6 56.645 58.086 1440.7 0.1507 - Averages 10089.6 4.0 4.1 4.1 7.8 280.9 620.61615 1.10 0.95 33.67 9622.5 4.357 4.468 110.8 0.0116 100.1 Comments: Replaced Elapsed time indicator on 711112016 Insert weekly flow cbeck values in,yellow columns. .. --~--.. ~ ~ -l . ..l.... Greeo columos are113lculo.ted.n,-ernges from· the mct'station. ~ ............... ~ .... ..:-.... --; Energey Fuels Resources -White Mesa Mill Calibration Date: 7n/2016 FirSt Momtoring Quarter 2014 :BHV-7 Period: September 27th, 2016-December 27th, 2016 Calibration Slope & Intercept: m= 1.25008 b= -0.0206 Updated: 7/30/14 -~"' -Orifice SIN: 8091779 till l!.H 0 -IUf. 0 0 T<~ Tl P.n :~,·, Q\· -... ~. . :;Fcib1' -II -~ --~ .. Week Filter Start Stop Start Stop r~ Starting Stopping A~ \Vlii~.JIIvg: ~~-~ ·WKly. Avg. ~:~; ·~--~~~' I .. I ~I I-~ _Ne(. '':~~~ ;~n ~ .. -... -... -.' , -•.; • ~ ~ I .$!4-'~ # Number Date Date Time Time ~ Manomete~ Manometer Tern~;>. -T~·-, .Ptessure ' .... I ~' ~~-,,, I L~ I :cllliD) (in. H20) (in. H20) :<.i!t.ltP>. ~~) ~1 (oimHg) :(il(*) l,{~~· -~~)' ....,;.~I I Jg J£...tl!l!l' ,,(i.ia'!i_ey;: -~1(ttl I 9220199 9/27/2016 10/3/2016 14123.69 14267.53 8630.4 4,0 4.0 4.0 16.1 289.2 622.30 1.11 0.93 32.99 8061.3 4.3116 4.3788 67.2 0.0083 85.6 2 9220188 10/3/2016 10110/2016 14267.53 14438.11 10234.8 4.0 4.0 4.0 11.5 284.6 620.26 1.10 0.94 33.20 9622.1 4.3537 4,4614 107.7 0.0112 101.5 3 9220180 10/10/2016 10/17/2016 14438.11 14602 9833.4 4.0 ;4.0 4.0 15.8 289.0 619.76 1.11 0.93 32.93 9170.3 4.3272 4.5187 191.5 0.0209 97.6 4 9220175 10117/2016 10/2412016 14602 14770.64 10118.4 4.0 4.0 4.0 12.6 285.7 621.79 1.10 0.94 33.18 9506.5 4.3492 4.5210 171.8 0.0181 100.4 5 9220164 10/24/2016 10/31/2016 14770.64 14938.35 10062.6 4.0 4.0 4.0 14.3 287.5 622.6 1.10 0.94 33.10 9430.1 4.3432 4.4507 107.5 0.0114 99.8 I 6 9220159 10/31/2016 1117/2016 14938.35 15106.95 10116 4.0 4.0 4.0 11.2 284.3 621.79 1.10 0.94 33.26 9527.4 4,3436 4.4274 83.8 0.0088 100.4 7 9220151 1117/2016 11114/2016 15106.95 15275.67 10123.2 4.0 4.0 4.0 9.4 282.6 624.84 1.09 0.95 33.45 9587.8 4.3586 4.4634 104.8 0.0109 100.4 8 9220139 11/14/2016 11/21/2016 15275.67 15442.91 10034.4 4,0 4.0 4.0 6.9 280.1 620.77 1.09 0.95 33.49 9515.2 4.3661 4.5644 198.3 0.0208 99.5 9 9220131 11121/2016 11/28/2016 15442.91 15611.2 10097.4 4.0 4.0 4.0 3.3 276.4 619.50 1.09 0.95 33.68 9629.4 4.3718 4.4457 73.9 0.0077 100.2 10 9220124 11/28/2016 1215/2016 15611.2 15780.03 10129.8 4.0 4.0 4.0 -1.2 271.9 616.96 1.08 0.96 33.89 9720.5 4.3309 4.3785 47.6 0.0049 100.5 I I 9220119 1215/2016 1211212016 15780.03 15947.12 10025.4 4.0 4,0 4.0 0.8 273.9 618.99 1.08 0.96 33.82 9600.9 4.3907 4.4723 81.6 0.0085 99.5 12 9220107 1211212016 12119/2016 15947.12 16120.08 10377.6 4.0 4.0 4.0 1.3 274.4 618.49 1.08 0.96 33.77 9924.2 4.3886 4.5079 119.3 0.0120 103.0 13 9220100 12/19/2016 12127/2016 16120.08 16310.77 11441.4 4.0 4.0 4.0 -1.0 272.1 620.01 1.08 0.96 33.96 I 1002.7 4.3114 4.3784 67.0 0.0061 I 13.5 Totals 131224.8 14.21 12.31 434.7 1 124298.3 56.547 57.969 1422.0 0.1496 Averages 10094.2 4.0 4.0 4.0 7.8 280.9 620.61615 1.09 0.95 33.44 9561.4 4.350 4.459 109.4 0.0115 100.1 Comments: Insert weekly flow check values in yellow columns. ~----... __:_,.,_. ,;'.-·) _ _. .· . -. j Green C'OlumnS'ate.ca1crulated averages from 1M met station.. . ·C. •. •· , -,-~li'iiii'"" -J Energey Fuels Resources -White Mesa Mill Calibration Date: 717/2016 First Monitoring Quarter 2014 BHV-8 Period: September 27th, 2016-December 27th, 2016 Calibration Slope & Intercept: m= 1.25008 b= -0.0206 Updated: 7/30/14 Orifice SIN: 8091779 llli llli •• rt:a . 'TO: Th ~-~ I . :c:tr• -.~ . QS --I .;.TOail; .· --I . -. -.., I ~ I i-~· ~-. .I Week Filter Start Stop Start Stop T'«al Starting Stopping I ·~~-Wkli. 1'-:v&, ~-A~ Wkb'.A,•g'. -~ •SMt'fiOW; .Sii.'~' : •sit; A J' \·~·· .··_ Nirt l:~i' ~: ·~ '" ~---· -..... -~ j--1,T ..~~· lt. ·· . .> • ~ .... '1 # Number Date Date Time Time Manometer ~anometer Temp. T~ lh=ure -, ... ~ti!!L (in. H20) (in. H20) (In;;~~ ("€> ®:· (mn!Hg} ' (liltmiol: l~~)j' _ .. n~ . ..tit'_' ":Z -~·r , !.Cftl' . J .. : 'J I 9220200 9/27/2016 10/3/2016 501.25 645.6 8661 4.0 3.5 3.8 16.1 289.2 622.30 1.07 0.90 31.95 7836.8 4.3238 4.3696 45.8 0.0058 85.9 2 9220187 10/3/2016 10110/2016 645.Q 816.28 10240.8 4.0 4.0 4.0 11.5 284.6 620.26 1.10 0.94 33.20 9627.8 4.3757 4.4289 53.2 0.0055 101.6 3 9220179 10110/2016 10117/2016 816.28 967.98 9102 4.0 4.0 4.0 15.8 289.0 619.76 1.11 0.93 32.93 8488.2 4.2938 4.3860 92.2 0.0109 90.3 4 9220176 10/17/2016 10/24/2016 967.98 1137.3 10159.2 4.0 3.5 3.8 12.6 285.7 621.79 1.07 0.91 32.14 9246.3 4.3316 4.4630 131.4 0.0142 100.8 5 9220163 10/24/2016 10/31/2016 1137.3 1304.19 10013.4 4.0 3.0 3.5 14.3 287.5 622.6 1.03 0,88 30.99 8787.0 4.3239 4.3774 53.5 0.0061 99.3 6 9220160 10/31/2016 1117/2016 1304.19 1473.29 10146 4.0 4.0 4.0 11.2 284.3 621.79 1.10 0.94 33.26 9555.7 4.3437 4.3970 53.3 0.0056 100.7 7 9220152 1117/2016 11/14/2016 1473.29 1627.69 9264 4.0 4.0 4.0 9.4 282.6 624.84 1.09 0.95 33.45 8774.0 4.3367 4.4014 64.7 0.0074 91.9 8 9220138 11/14/2016 ll/21/2016 1627.69 1794.5 10008.6 4.0 4.0 4.0 6.9 280.1 620.77 1.09 0.95 33.49 9490.7 4.3023 4.4591 156.8 0.0165 99.3 I 9 9220130 ll/21/2016 ll/28/2016 1794.5 1948.1 9216 4.0 4.0 4.0 3.3 276.4 619.50 1.09 0.95 33.68 8788.8 4.3813 4.4459 64.6 0.0074 91.4 10 9220123 ll/28/2016 1215/2016 1948.1 2116.92 10129.2 4.0 4.0 4.0 -1.2 271.9 616.96 1.08 0.96 33.89 9719.9 4.3309 4.3624 31.5 0.0032 100.5 II 9220120 12/5/2016 1211212016 2116.92 2284.39 10048.2 4.0 6.5 5.3 0,8 273.9 618.99 1.24 1.10 38.67 11002.9 4.3589 4.4262 67.3 0.0061 99.7 12 9220106 12112/2016 12119/2016 2284.39 2455.5 10266.6 3.5 4.0 3.8 1.3 274.4 618.49 1.05 0.93 32.72 9511.0 4.3707 4,4455 74.8 0.0079 101.9 13 9220099 12119/2016 12127/2016 2455.5 2616 9630 4.0 4.0 4.0 -1.0 272.1 620.01 1.08 0.96 33.96 9260.7 4.3150 4.3427 27.7 0.0030 95.5 I Totals 126885.0 14.19 12.30 434.33 120089.8 56.388 57.305 916.8 0.0996 Averages 9760.4 4.0 4.0 4.0 7.8 280.9 620.61615 1.09 0.95 33.41 9237.7 4.338 4.408 70.5 0.0077 96.8 Comments: Insert weekly flow check values in yellow columns. ~ • --;~.~· ...••• : ,;_-~-< =~~~;Jaul~j;~t~m I~ mC!stntism. Btaaks Penod: June 27th, 2016 -, June 27th 2016 Week Filter Start Stop Net # Number Date Date 1 9219790 27-Jun-16 05-Jul-16 4.3648 2 9219782 05-Jul-16 11-Jul-16 4.3795 3 9219781 11-Jul-16 18-Jul-16 4.3799 4 9219766 18-Jul-16 25-Jul-16 4.3621 5 9219765 25-Jul-16 01-Aug-16 4.3598 6 9219750 01-Aug-16 08-Aug-16 4.3889 7 9219749 08-Aug-16 15-Aug-16 4.3762 8 9219734 15-Aug-16 22-Aug-16 4.3078 9 9219733 22-Aug-16 29-Aug-16 4.3572 10 9219718 29-Aug-16 06-Sep-16 4.3755 11 9219717 06-Sep-16 12-Sep-16 4.3829 12 9219702 12-Sep-16 19-Sep-16 4.3674 13 9219701 19-Sep-16 27-Sep-16 4.3999 Totals Blanks Penod: September 27th, 2016- December 27th 2016 Week Filter Start Stop Net # Number Date Date 1 9220186 27-Sep-16 03-0ct-16 4.3704 2 9220178 03-0ct-16 1 0-0ct-16 4.3097 3 9220177 10-0ct-16 17-0ct-16 4.3083 4 9220162 17-0ct-16 24-0ct-16 4.2955 5 9220161 24-0ct-16 31-0ct-16 4.3010 6 9220153 31-0ct-16 07-Nov-16 4.3456 7 9220145 07-Nov-16 14-Nov-16 4.3627 8 9220137 14-Nov-16 21-Nov-16 4.3152 9 9220122 21-Nov-16 28-Nov-16 4.3227 10 9220121 28-Nov-16 05-Dec-16 4.3425 11 9220113 05-Dec-16 12-Dec-16 4.3336 12 9220098 12-Dec-16 19-Dec-16 4.3539 13 9220090 19-Dec-16 27-Dec-16 4.3323 Totals ATTACHMENT E ENVIRONMENTAL GAMMA GRAPHS AND SUPPORTING DATA [White Mesa Mill Ambient Gamma Levels Over Time BHV-11 50.00 r----------------------------------------------------------------------------------------------------------------, 45.00 1_--------------------------------------------------------------------------------------------------------------------~ 40.00 +---------------------------------------------------------------------------------------------------------------_, 35.00 +---------------------------------------------------------------------------------------------------------------_, 30.00 .... ~ (tl ::I 25.00 ~ E (J) a: 20.00 E 15.00 10.00 +--------------------------------------------------------------11r--------------------------------------------4~-4 5.00 II • HH -HHH-IIM J\ II I 1 • 0.00 ,~... ... -.... ii¥ .,...-.• r ~ ~ . . • 1 9i30tt98t 9tao;t984 9tao;19B7 9i30ttg90 9!Jottgg3 9i30ttg96 9tao;t999 9taot.?002 9taol2oos 9taot.?008 9130t.?ott 9taol2o14 Background (BHV-3) Subtracted from BHV-1 I -~ I I White Mesa Mill Ambient Gamma Levels Over Time BHV-21 50.00 ~-----------------------------------------------------------------------------------------------------, 45.00 +-----------------------------------------------------------------------------------------------------_, 40.00 +-------------------------------------------------------------------------------------------------~ 35.00 +-----------------------------------------------------------------------------------------------------_, 30.00 .... Q) t:::: cu ::;) o-25.00 --E Q) a: E 20.00 15.00 +------------------------------------------------------------------------------------------------------4 10.00 +-------------~---------------------------------------------------------------------------------------4 5.00 I lr-II H. • -• J'f • 0.00 ........... , '" ··46 .... , 11'biei --.,.,.. .. ~-·v-:JAaP I ~' ~ . -• .,.,.,I,.. ~ I 3o.seP..8t 3o.sep..eg 30-sep.g1 3o.seP..os 30-sep..13 Background (BHV-3) Subtracted from BHV-2 ,---......-BHV-2 ----I I White Mesa Mill Ambient Gamma Levels Over Time BHV-3 1 60.00 ~------------------------------------------------------------------------------------------------------------------------~ 50.00 ~------------------------------------------------------------------------------------------------------------------------------ 40.00 .... CD t:: ro ::I C" 30.00 ..._ E CD a: E 20.00 10.00 ~ I 0.00 . : ~ ~ ~ ~ ~ ~ •s ~ ~ •s •s •s ~ •s •s •s •s •s 8P-Bt 8P-B3 8P-Bs 8P-B7 8P-B9 8P-9t 8P-93 8P-9S ep..97 8P-99 8P·Ot 8P·03 ""P-Os 8P-07 8P·09 8P-1t 8P-13 8P.ts -BHV-3 I White Mesa Mill Ambient Gamma Levels Over Time BHV-41 50.00.------------------------------------------------------------------------------------------------, 45.00 +----------------------------------------------------------------------------------------------------4 40.00 +----------------------------------------------------------------------------------------------------4 35.oo I 30.00 +------------------------------------------------------------------------------------------------4 ~ ID ~ 25.00 ,--------------------------------------------------------------------------------------------- ~ 1 , .. 00~-------------------------------------------------------------------------------------- 15.00 I 10.00 +-_,+-----------------------------------------------------------------------------------------------~ 5.oo I •1 .llf • II II • 1\-----1 iA • ---0.00 I 3o.seP-8t 3D-sep-84 30-seP-87 30-sep.9o 30-seP-93 30-sep.96 3o..seP-99 30-sep.o2 3o-seP-os 3o..seP-OB 3o.sep.11 30-sep.14 Background (BHV-3) Subtracted from BHV-4 [ ~BHV-4 I I White Mesa Mill Ambient Gamma Levels Over Time BHV:sl 50.00~-------------------------------------------------------------------------------------------, 45.00 +--------------------------------------------------------------------------------------------1 40.00 +------------------------------------------------------------------------------------------------; 35.00 +-------------------------------------------------------------------------------------------_, 30.00 ..... Q) t ctS ::J 0" 25.00 -E Q) a: E 20.00 15.00 +------------------------------------------------------------------------------------------------; 10.00 ~ 5.00 I I I t• -.. 1-.. nJ'l I~ I I a .,... I I 1 \---H;.-1 1 'Ill' I Ill 11 ·:.1...-~·H---l--l o.oo •• -, =-· M ·• e • • , e ·• .• _.. , , • 30-Sep-a1 ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ 'P-84 'P-8 1 'P-9o 'P-93 'P-96 'P-99 'P-0< 'P-Os 'P-Oe 'P-11 'P-14 Background (BHV-3) Subtracted from BHV-5 I ....._BHV-5 I I White Mesa Mill Ambient Gamma Levels Over Time BHV-61 50.00 45.00 40.00 35.00 30.00 '-<I> t::: (lj 25.00 :::l C" --E <I> a: 20.00 E 15.00 10.00 . ~ " .~ ,. AA -~ l.Jl! ~. --------- 5.00 0.00 3o.Sep-fJ1 30-Sep-84 3o.seP-8? 30-Sep.go 3o.Sep.93 3o.Sep.96 3o.Sep.99 30-sep-o2 30-seP-o5 30-sep-o8 30-sep.11 30-sep.14 Background (BHV-3) Subtracted from BHV-6 I -~ I I White Mesa Mill Ambient Gamma Levels Over Time BHV-71 50.00 45.00 40.00 35.00 30.00 ..... Q) t:: ca 25.00 ::I C" ...._ E Q) a: 20.00 E 15.00 10.00 ~ -J ~-/ -. -. . '-. '---. . 5.00 0.00 1-SeP-14 1-fVov-14 1van-ts 1-Mar-ts 1-May.1S 1vul-ts 1-Sep.1s 1-Nov.ts 1van.16 1-Mar-16 1·May.16 1-Jui-16 1-Sep.16 1-Nov-16 1-Jan-17 Background (BHV-3) Subtracted from BHV-7 I -~ I I White Mesa Mill Ambient Gamma Levels Over Time BHV-81 50.00 45.00 40.00 35.00 30.00 .... Q) t::: co 25.00 :::::l 0" ........ E Q) c: 20.00 E 15.00 ~ ---J ~---_. ----------- 10.00 5.00 0.00 1-SeP-14 1-tvo"'-14 1-Jan-1s 1-f1.1ar-1s 1·11.1ay.ts 1-Juf-1s 1-SeP-1s 1-tvo.,._1S 1-Jan-16 1-Mar-16 1-f1.1ay.16 1-Juf-16 1-SeP-16 1-tvo"'-16 1-Jan-17 Background (BHV-3) Subtracted from BHV-8 I -~ I Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 51 52 53 64 70 71 White Mesa Mill Third Quarter 2016 Environmental Spherical Gamma Monitor Results Mean Location Administration Vault V205 Control Room BHV-6 Date Issued Date Returned Ore Stor. -Barrel Area Vanadium Precip.Area Yellowcake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room )re pad -decontamination pa• North East Corner Ore Pad Met. Lab Filter Press Room BHV-1 BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scalehouse Sample Plant (OBS) 717/2016 717/2016 717/2016 717/2016 7/7/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 717/2016 Front Gate 7/7/2016 AF-Barrel Dump Station 717/2016 AF Circuit-South 717/2016 AF Circuit-North 717/2016 North Control# 1 717/2016 North Control# 2 717/2016 CaF2 Barrel Dump Station - Operator Station 7/7/2016 KF Barrel Dump Station 7/7/2016 BHV-7 717/2016 BHV-8 717/2016 10/10/2016 10110/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10110/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 Total Days Badge at WMM 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 Ambient Dose Equivalent 38.5 64.5 39.9 221 119.3 348.3 274.7 331.6 210.1 84.9 163.3 342.4 95.3 168 46.6 43.4 41.6 40.9 40 350.3 83.5 98.1 115.7 57.3 97.2 410.7 1065.4 185.7 79.6 142.3 67.7 384.4 223.2 266.7 216.1 171.4 267.3 94.3 54.2 40.4 129.1 261.9 39.5 42.4 mRem/ hour 0.02 0.03 0.02 0.10 0.05 0.15 0.12 0.15 0.09 0.04 0.07 0.15 0.04 0.07 0.02 0.02 0.02 0.02 0.02 0.15 0.04 0.04 0.05 0.03 0.04 0.18 0.47 0.08 0.03 0.06 0.03 0.17 0.10 0.12 0.09 0.08 0.12 0.04 0.02 0.02 0.06 0.11 0.02 0.02 mRem/Day 0.405 0.679 0.420 2.326 1.256 3.666 2.892 3.491 2.212 0.894 1.719 3.604 1.003 1.768 0.491 0.457 0.438 0.431 0.421 3.687 0.879 1.033 1.218 0.603 1.023 4.323 11.215 1.955 0.838 1.498 0.713 4.046 2.349 2.807 2.275 1.804 2.814 0.993 0.571 0.425 1.359 2.757 0.416 0.446 mRem/ Week 2.84 4.75 2.94 16.28 8.79 25.66 20.24 24.43 15.48 6.26 12.03 25.23 7.02 12.38 3.43 3.20 3.07 3.01 2.95 25.81 6.15 7.23 8.53 4.22 7.16 30.26 78.50 13.68 5.87 10.49 4.99 28.32 16.45 19.65 15.92 12.63 19.70 6.95 3.99 2.98 9.51 19.30 2.91 3.12 Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 51 52 53 64 70 71 White Mesa Mill Fourth Quarter 2016 Environmental Spherical Gamma Monitor Results Location Administration Vault V205 Control Room BHV-6 Ore Stor. -Barrel Area Vanadium Precip.Area Yellowcake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room )re pad -decontamination pa< North East Corner Ore Pad Met. Lab Filter Press Room BHV-1 BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scalehouse Sample Plant (OBS) Front Gate AF -Barrel Dump Station AF Circuit -South AF Circuit-North North Control# 1 North Control# 2 CaF2 Barrel Dump Station - Operator Station KF Barrel Dump Station BHV-7 BHV-8 Date Issued Date Returned 10110/2016 10/10/2016 10/10/2016 10/10/2016 10110/2016 10/10/2016 10110/2016 10110/2016 10/10/2016 10110/2016 10110/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10110/2016 10/10/2016 10110/2016 10/10/2016 10/10/2016 10110/2016 10/10/2016 10110/2016 10110/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10110/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10110/2016 10/10/2016 10/10/2016 10/10/2016 10/10/2016 10110/2016 10/10/2016 10110/2016 10/10/2016 10110/2016 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 113/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 113/2017 113/2017 1/3/2017 113/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 113/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 113/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 1/3/2017 Total Days Badge at WMM 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 85 Mean Ambient Dose Equivalent 42.2 50.5 34.6 402.8 121.8 304.5 198.8 267.8 200.6 88.3 131 270 88.3 152.9 38.2 39 34.2 35.4 36.3 281.5 38.8 139.5 95.4 43.9 77.1 364.3 782.8 94 56.4 140.8 50.1 374.5 199.4 179.3 180.5 246.2 318.2 138.2 40.2 36.7 104.5 248.8 38.5 36 mRem/ hour 0.02 0.02 0.02 0.20 0.06 0.15 0.10 0.13 0.10 0.04 0.06 0.13 0.04 0.07 0.02 0.02 0.02 0.02 0.02 0.14 0.02 0.07 0.05 0.02 0.04 0.18 0.38 0.05 0.03 0.07 0.02 0.18 0.10 0.09 0.09 0.12 0.16 0.07 0.02 0.02 0.05 0.12 0.02 0.02 mRem/Day 0.496 0.594 0.407 4.739 1.433 3.582 2.339 3.151 2.360 1.039 1.541 3.176 1.039 1.799 0.449 0.459 0.402 0.416 0.427 3.312 0.456 1.641 1.122 0.516 0.907 4.286 9.209 1.106 0.664 1.656 0.589 4.406 2.346 2.109 2.124 2.896 3.744 1.626 0.473 0.432 1.229 2.927 0.453 0.424 mRem/ Week 3.48 4.16 2.85 33.17 10.03 25.08 16.37 22.05 16.52 7.27 10.79 22.24 7.27 12.59 3.15 3.21 2.82 2.92 2.99 23.18 3.20 11.49 7.86 3.62 6.35 30.00 64.47 7.74 4.64 11.60 4.13 30.84 16.42 14.77 14.86 20.28 26.20 11.38 3.31 3.02 8.61 20.49 3.17 2.96 ATTACHMENT F VEGETATION GRAPHS, DATA TABLE, LABORATORY RESULTS AND QAJQC {Log Scale) ...... ...... ...... ...... ...... ...... ...... 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I 6 I 0 0 0 0 0 0 co ...... (J) (11 .j::. w 1\) 8/27/1981 8/27/1982 8/27/1983 8/27/1984 8/27/1985 8/27/1986 8/27/1987 8/27/1988 8/27/1989 ::0 8/27/1990 D) I 1\) 8/27/1991 1\) Q) 8/27/1992 0 0 ::::J 8/27/1993 (') CD 8/27/1994 ::::J -""' 8/27/1995 -D) - f s· 8/27/1996 ::::J 0 z 8/27/1997 ::::J m 8/27/1998 < CD f 8/27/1999 cc CD -8/27/2000 D) z -~ s· 8/27/2001 ::::J -f 8/27/2002 c 0 8/27/2003 ::::::.: (/) " ~ cc 8/27/2004 - 8/27/2005 8/27/2006 8/27/2007 8/27/2008 8/27/2009 8/27/2010 8/27/2011 8/27/2012 8/27/2013 - 8/27/2014 8/27/2015 8/27/2016 (Log Scale} _. _. _. _. _. _. _. 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 OJ -....! 0) 01 """' w 1\) 8/27/1981 8/27/1982 8/27/1983 8/27/1984 8/27/1985 8/27/1986 8/27/1987 8/27/1988 8/27/1989 "'C 8/27/1990 C" I 1\) 8/27/1991 ..... 0 8/27/1992 0 0 8/27/1993 ~ n CD 8/27/1994 ~ -.., 8/27/1995 D) -t 5' 8/27/1996 ~ 0 z 8/27/1997 ~ m 8/27/1998 < CD f 8/27/1999 cg CD -8/27/2000 -D) z -::E s· 8/27/2001 ~ -t 8/27/2002 c: 0 8/27/2003 ::::::: (/) :::-r;; ::E cg 8/27/2004 - 8/27/2005 8/27/2006 8/27/2007 8/27/2008 8/27/2009 8/27/2010 8/27/2011 8/27/2012 8/27/2013 8/27/2014 - 8/27/2015 8/27/2016 9~0G/~/~ ~ 9~0cH/O~ 9~0G/~/6 9~0cH/8 9Wc/~/L 9~0GH/9 9~0G/~/9 -;: m ~ 9~0GH/v (/) f 0 :::J -9Wc/~J£ c ;: 0 ;: z ca 9~0G/~/G T G) m Cl) > 9~0G/~/~ w .5 z rn 9~0G/~/G~ 1 c 0 ;: ca ... 9WGHH~ -c Cl) u c 9WcHJO~ 0 0 ~ 9~0GH/6 z I ::J 9~0GH/8 9WG/~JL 9~0G/~/9 9~0G/~/9 9~0cH/v C\1 C') "<t It) (.() ,..._ CX> 0 0 0 0 0 0 0 . . w . I I w w w w w w 0 0 0 0 0 0 0 ~ ~ ~ ~ ~ ~ ~ (aiB:)S 601) (Log Scale) _. _. _. 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I 6 I 0 0 0 0 0 0 CXl -...j en (}1 """' VJ 1\) 4/1/2015 5/1/2015 6/1/2015 7/1/2015 8/1/2015 I I I II I I I I I -1 ::r:: I 9/1/2015 I I I II I I I I I "' w "' 0 10/1/2015 I I I It I I I I 0 ::::s (') (I) 11/1/2015 I I I .I • I I I ::::s -""'' m - f 12/1/2015 j 1\ cr ::::s t/) z S' m 1/1/2016 ~ f cc (I) 2/1/2016 -m z -:E o· 3/1/2016 ::::s -f c 0 4/1/2016 :::::: (/) " :E cc - 5/1/2016 6/1/2016 7/1/2016 8/1/2016 9/1/2016 10/1/2016 11/1/2016 WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHEAST OF MILL SAMPLED SAMPLED Ra-226 QTR. DATE VALUE (uCi/Kg) 3rd '81 27-Aug-81 3.90E-04 4th '81 20-0ct-81 1.40E-04 2nd '82 15-Apr-82 1.31E-04 3rd '82 01-Jul-82 1.60E-04 4th '82 30-Nov-82 2.67E-06 2nd '83 13-Apr-83 9.36E-05 3rd '83 01-Jul-83 1.12E-04 4th '83 30-Jan-84 1.09E-04 2nd '84 28-Jun-84 3.47E-04 4th '84 14-Nov-84 5.61E-04 2nd '85 27-Mar-85 1.05E-03 3rd '85 15-Jul-85 8.20E-05 4th '85 09-0ct-85 1.15E-04 2nd '86 24-Mar-86 5.72E-04 3rd '86 10-Jul-86 5.01E-04 4th '86 18-Dec-86 8.70E-04 2nd '87 20-Apr-87 5.90E-04 3rd '87 05-Jun-87 1.60E-04 4th '87 22-Dec-87 2.10E-04 2nd '88 19-Apr-88 4.50E-04 3rd '88 28-Jul-88 3.20E-05 2nd '89 07-Apr-89 5.60E-04 3rd '89 06-Jun-89 1.50E-04 4th '89 07-Nov-89 6.00E-04 1st '90 17-Apr-90 2.60E-04 2nd '90 20-Jun-90 1.80E-04 3rd '90 17-0ct-90 1.60E-04 1st '91 10-Apr-91 1.20E-04 2nd'91 11-Jun-91 9.10E-05 3rd '91 20-Nov-91 4.50E-04 1st '92 22-Apr-92 3.60E-05 2nd'92 10-Jun-92 l.OOE-05 3rd '92 10-Jun-92 7.90E-05 1st '93 13-Apr-93 3.70E-05 2nd'93 26-Jun-93 3.00E-05 3rd '93 12-0ct-93 6.60E-05 1st '94 11-May-94 l.80E-04 2nd '94 19-Jul-94 l.71E-05 3rd '94 28-Nov-94 2.40E-04 1st '95 11-Apr-95 6.70E-05 2nd'95 06-Jul-95 1.50E-05 3rd '95 15-Nov-95 5.50E-05 1st '96 23-Apr-96 5.20E-05 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 3.00E-05 1st '97 21-Apr-97 l.IOE-05 3rd '97 05-Sep-97 l.IOE-05 4th '97 20-Nov-97 8.00E-06 1st '98 23-Mar-98 <9.10E-05 2nd '98 16-Jun-98 1.80E-05 4th '98 05-Nov-98 5.70E-05 2nd'99 15-Apr-99 2.00E-04 3rd '99 07-Jul-99 6.03E-05 4th '99 02-Dec-99 2.30E-05 2nd '00 21-Apr-00 1.50E-04 2nd '00 22-Jun-00 1.20E-06 4th '00 21-Dec-00 l.60E-06 1st '01 30-Apr-01 l.OOE-06 2nd 'OJ 14-Jun-01 2.30E-06 4th '01 17-Dec-01 9.10E-06 1st '02 07-May-02 3.30E-05 2nd '02 07-Jul-02 5.55E-05 4th '02 15-Dec-02 7.75E-05 Ra-226 MDC¥ Pb-210 Pb-210 ERROR LLD uCi/Kg VALUE ERROR (uCi/Kg) (S.OE-08) (uCi/Kg) (uCi/Kg) l.OOE-05 5.00E-08 l.IOE-03 l.OOE-04 l.OOE-05 5.00E-08 6.80E-04 8.00E-05 1.30E-05 I.OOE-06 4.90E-04 7.00E-05 l.OOE-05 5.00E-08 8.00E-04 1.70E-04 1.07E-06 I.OOE-06 1.08E-04 9.00E-06 6.20E-06 8.00E-09 4.97E-04 9.30E-05 1.20E-05 6.00E-06 1.84E-04 l.20E-05 8.00E-06 4.00E-06 7.80E-04 6.20E-05 1.20E-05 2.00E-09 3.75E-03 l.60E-04 l.99E-04 2.00E-07 7.82E-03 3.30E-04 3.00E-05 2.00E-06 3.22E-03 l.40E-04 7.00E-06 3.00E-06 7.70E-04 1.30E-04 l.OOE-05 3.00E-06 5.10E-04 3.00E-05 2.10E-05 4.00E-06 2.49E-03 l.OOE-04 1.30E-05 3.00E-06 1.57E-03 1.70E-03 5.00E-05 3.00E-06 6.80E-04 3.00E-05 7.00E-05 5.00E-08 1.50E-03 1.00E-04 3.00E-05 5.00E-08 9.50E-04 4.00E-05 4.00E-05 5.00E-08 1.70E-03 1.00E-04 7.00E-05 5.00E-08 1.40E-03 l.OOE-04 2.20E-05 5.00E-08 1.50E-04 4.40E-04 4.00E-05 *** l.IOE-03 l.OOE-01 2.00E-05 *** 2.30E-04 2.00E-05 5.00E-05 7.00E-06 2.04E-03 7.00E-05 3.00E-05 4.00E-06 3.30E-04 2.00E-05 2.00E-05 5.00E-08 3.20E-04 2.00E-05 2.00E-05 5.00E-08 3.30E-04 2.00E-05 2.00E-05 5.00E-06 3.00E-04 2.00E-05 1.60E-05 2.00E-07 1.90E-04 2.00E-05 4.00E-05 5.00E-08 l.09E-03 5.00E-05 l.OOE-05 2.00E-06 l.50E-04 2.00E-05 ?.OOE-06 2.00E-07 7.50E-05 2.00E-05 3.50E-05 3.00E-06 7.10E-04 7.00E-05 2.20E-05 3.00E-06 2.80E-04 3.00E-05 l.50E-05 3.00E-06 4.30E-05 3.50E-05 2.70E-05 3.00E-06 5.30E-04 6.00E-05 4.00E-05 3.00E-05 4.40E-04 6.00E-05 1.20E-06 9.00E-08 3.00E-05 6.10E-06 1.50E-05 1.70E-07 !.70E-04 l.10E-05 5.40E-06 l.60E-07 1.40E-04 1.30E-05 1.50E-06 1.50E-07 5.10E-05 4.50E-06 5.00E-06 1.80E-07 6.70E-05 l.OOE-05 2.50E-06 l.50E-07 3.20E-05 4.50E-06 2.50E-06 1.80E-07 l.40E-04 7.10E-06 4.70E-07 l.21E-07 4.10E-05 3.60E-06 4.30E-07 1.33E-07 2.10E-05 7.30E-07 1.20E-06 5.60E-07 1.40E-04 4.60E-06 9.10E-05 9.10E-05 <4.50E-04 4.50E-04 l.20E-06 6.30E-08 4.00E-05 1.80E-06 l.OOE-06 8.20E-08 8.70E-05 5.00E-06 3.00E-06 1.20E-07 3.00E-04 l.OOE-05 1.40E-06 8.30E-08 1.40E-04 4.70E-06 1.00E-06 2.30E-07 2.10E-05 I.OOE-06 3.00E-06 1.20E-07 1.60E-04 S.OOE-06 l.OOE-07 2.80E-07 l.60E-04 l.OOE-05 l.lOE-06 3.70E-07 5.10E-05 5.00E-06 l.OOE-07 2.40E-07 <l.2E-06 l.OOE-07 2.00E-07 9.90E-08 3.80E-06 2.00E-07 2.40E-06 1.20E-07 3.57E-05 2.97E-06 1.80E-06 7.60E-07 4.50E-05 2.61E-06 2.81E-06 7.60E-07 5.31E-05 3.90E-06 3.60E-06 7.60E-07 1.29E-04 6.15E-06 MDC¥ U-N AT U-NAT MDC¥ Th-232 Th-232 MDC¥ LLDuCi/Kg VALUE ERROR LLD VALUE ERROR LLD (l.OE-06) (uCi/Kg) (uCi/Kg) uCi/Kg (uCi/Kg) (uCi/Kg) uCi/Kg (2.0E-07) (2.0E-07)t l.OOE-06 NS NA NA NS NA NA l.OOE-06 NS NA NA NS NA NA 8.00E-05 NS NA NA NS NA NA I.OOE-07 NS NA NA NS NA NA I.OOE-05 NS NA NA NS NA NA I.OOE-04 NS NA NA NS NA NA I.OOE-06 NS NA NA NS NA NA 6.00E-05 NS NA NA NS NA NA 4.00E-08 NS NA NA NS NA NA 7.00E-08 NS NA NA NS NA NA 2.00E-05 NS NA NA NS NA NA 2.00E-04 NS NA NA NS NA NA 2.00E-05 NS NA NA NS NA NA I.OOE-05 NS NA NA NS NA NA 2.00E-04 NS NA NA NS NA NA 3.00E-06 NS NA NA NS NA NA I.OOE-06 NS NA NA NS NA NA I.OOE-06 NS NA NA NS NA NA I.OOE-06 NS NA NA NS NA NA !.OOE-06 NS NA NA NS NA NA l.OOE-06 NS NA NA NS NA NA *** NS NA NA NS NA NA *** NS NA NA NS NA NA 1.40E-05 NS NA NA NS NA NA 2.20E-05 NS NA NA NS NA NA l.OOE-06 NS NA NA NS NA NA l.OOE-06 NS NA NA NS NA NA I.OOE-06 NS NA NA NS NA NA 2.00E-07 NS NA NA NS NA NA l.OOE-06 NS NA NA NS NA NA l.OOE-05 NS NA NA NS NA NA l.OOE-06 NS NA NA NS NA NA 2.00E-05 NS NA NA NS NA NA 2.00E-05 NS NA NA NS NA NA 2.00E-05 NS NA NA NS NA NA 2.00E-05 NS NA NA NS NA NA 2.00E-04 NS NA NA NS NA NA 4.45E-06 NS NA NA NS NA NA 8.30E-07 NS NA NA NS NA NA 7.90E-07 NS NA NA NS NA NA 7.60E-07 NS NA NA NS NA NA 8.80E-07 NS NA NA NS NA NA 1.80E-07 NS NA NA NS NA NA NS NA NA NS NA NA 9.30E-07 NS NA NA NS NA NA 6.10E-07 NS NA NA NS NA NA 6.66E-07 NS NA NA NS NA NA l.IOE-07 NS NA NA NS NA NA 4.50E-04 NS NA NA NS NA NA 3.20E-07 NS NA NA NS NA NA 4.10E-07 NS NA NA NS NA NA 6.00E-05 NS NA NA NS NA NA 4.20E-07 NS NA NA NS NA NA l.lOE-06 NS NA NA NS NA NA 5.90E-07 NS NA NA NS NA NA 1.40E-06 NS NA NA NS NA NA l.90E-06 NS NA NA NS NA NA 2.40E-07 NS NA NA NS NA NA 5.00E-07 NS NA NA NS NA NA 6.00E-07 NS NA NA NS NA NA l.OOE-05 NS NA NA NS NA NA l.OOE-05 NS NA NA NS NA NA l.OOE-05 NS NA NA NS NA NA SAMPLED SAMPLED Ra-226 Ra-226 MDC¥ Pb-210 Pb-210 MDC¥ U-NAT U-NAT MDC¥ Th-232 QTR. DATE VALUE ERROR LLDuCi/Kg VALUE ERROR LLD uCi/Kg VALUE ERROR LLD VALUE (uCi/Kg) (uCi/Kg) (S.OE-08) (uCi/Kg) (uCi/Kg) (l.OE-06) (uCi/Kg) (uCi/Kg) uCi/Kg (uCi/Kg) (2.0E-07) 1st '03 21-Mar-03 9.10E-06 1.30E-06 3.60E-07 1.13E-05 1.61E-06 3.36E-06 NS NA NA NS 2nd '03 10-Jun-03 2.50E-05 1.30E-06 3.60E-07 3.26E-06 2.00E-06 7.38E-08 NS NA NA NS 4th '03 20-Nov-03 5.70E-05 3.50E-06 1.50E-07 4.05E-05 5.82E-06 8.30E-07 NS NA NA NS 1st '04 08-Apr-04 9.38E-05 3.70E-06 l.IOE-07 5.88E-05 3.00E-06 5.50E-07 NS NA NA NS 2nd '04 12-Jun-04 5.63E-05 3.40E-06 1.80E-07 6.42E-05 5.90E-06 9.00E-07 NS NA NA NS 4th '04 30-Nov-04 8.41E-05 5.50E-06 2.00E-08 2.48E-04 1.40E-05 3.00E-07 NS NA NA NS 1st '05 21-Apr-05 5.60E-05 3.00E-06 1.40E-07 5.80E-05 4.00E-06 6.90E-07 NS NA NA NS 2nd '05 13-Jun-05 9.10E-06 1.50E-06 1.80E-07 l.IOE-05 1.20E-05 9.00E-07 NS NA NA NS 4th '05 10-Nov-05 6.00E-05 3.00E-06 l.IOE-10 1.70E-06 6.40E-07 5.50E-10 NS NA NA NS 1st '06 03-Apr-06 8.00E-05 5.00E-06 5.00E-08 3.40E-04 1.20E-05 l.OOE-06 NS NA NA NS 2nd '06 16-Jun-06 4.10E-05 3.10E-06 S.OOE-08 1.16E-04 6.10E-06 l.OOE-06 NS NA NA NS 4th '06 28-Nov-06 1.17E-04 4.60E-06 1.90E-07 3.28E-04 9.50E-06 9.50E-07 NS NA NA NS 1st '07 30-Mar-07 9.70E-05 4.40E-06 1.90E-07 3.40E-04 8.70E-06 8.4-07 NS NA NA NS 2nd '07 1-Jun-07 1.30E-05 1.60E-06 1.90E-07 1.20E-04 6.60E-06 9.70E-07 NS NA NA NS 4th '07 23-Nov-07 7.00E-05 8.20E-06 2.00E-07 5.00E-04 2.00E-05 1.20E-06 NS NA NA NS 1st '08 22-Apr-08 3.60E-06 3.00E-06 5.20E-07 2.30E-04 1.40E-05 l.OOE-06 NS NA NA NS 2nd '08 18-Jun-08 3.20E-05 3.20E-06 1.80E-06 6.90E-05 3.50E-05 5.50E-05 NS NA NA NS 4th '08 12-Dec-08 1.50E-04 5.20E-06 9.90E-07 3.60E-04 2.90E-05 3.90E-05 NS NA NA NS 1st '09 28-Apr-09 5.90E-04 1.35E-05 1.50E-06 3.40E-04 1.30E-05 1.50E-06 NS NA NA NS 2nd '09 17-Jun-09 1.90E-05 1.45E-06 4.90E-07 3.60E-05 1.10E-05 1.80E-05 NS NA NA NS 4th '09 18-Dec-09 l.?OE-04 5.90E-06 4.80E-04 1.20E-05 NS NA NA NS 1st '10 13-May-10 2.2DE-04 7.20E-06 l.IOE-06 1.90E-04 1.90E-05 2.90E-05 NS NA NA NS 2nd '10 18-Jun-10 6.50E-05 3.40E-06 7.60E-07 1.40E-04 1.90E-05 2.90E-05 NS NA NA NS 4th '10 20-Dec-10 2.30E-05 1.70E-06 5.20E-07 l.OOE-05 1.50E-06 2.30E-06 NS NA NA NS 2nd 'II 23-Jun-11 2.40E-07 1.40E-07 1.80E-07 <2.9E-06 1.70E-06 2.90E-06 NS NA NA NS 3rd 'II 27-Jul-11 4.90E-06 6.30E-07 3.20E-07 9.50E-05 2.10E-06 2.50E-06 NS NA NA NS 4th 'II 23-Nov-11 7.20E-06 7.50E-07 2.90E-07 8.80E-08 4.30E-07 7.20E-07 NS NA NA NS 2nd '12 11-Apr-12 4.40E-05 1.90E-06 3.60E-07 2.10E-04 2.00E-06 l.OOE-06 NS NA NA NS 3rd '12 11-Jun-12 2.20E-05 8.40E-07 1.10E-07 1.30E-04 7.60E-06 5.90E-06 NS NA NA NS 4th '12 06-Nov-12 3.10E-05 4.82E-07 4.63E-08 4.26E-04 3.72E-06 6.52E-07 NS NA NA NS 2nd '13 30-Apr-13 1.14E-04 1.74E-06 5.34E-07 2.65E-04 4.41E-06 5.37E-06 NS NA NA NS 3rd '13 20-Jun-13 8.91E-05 2.16E-06 1.42E-06 1.42E-04 3.68E-06 6.17E-06 NS NA NA NS 4th '13 14-Nov-13 1.37E-04 3.87E-06 4.71E-06 5.33E-04 1.45E-05 2.27E-05 NS NA NA NS 2nd '14 16-Apr-14 9.90E-05 l.OIE-06 3.91E-07 1.99E-04 3.14E-06 3.38E-06 NS NA NA NS 3rd '14 10-Jun-14 2.60E-05 8.46E-07 9.19E-07 5.60E-05 3.08E-06 7.12E-06 NS NA NA NS 4th '14 25-Nov-14 2.98E-05 1.23E-06 1.30E-06 2.46E-04 5.38E-06 7.41E-06 NS NA NA NS 1st '15 21-Apr-15 7.15E-04 8.01E-06 3.50E-06 5.85E-04 1.27E-05 2.51E-05 6.36E-04 2.70E-05 8.62E-06 l.OIE-04 2nd '15 15-Jun-15 1.52E-04 3.48E-06 2.60E-06 4.49E-04 1.50E-05 3.33E-05 3.11E-04 1.58E-05 6.45E-06 4.19E-05 4th '15 23-Nov-15 2.34E-04 5.79E-06 3.89E-06 9.34E-04 1.36E-05 1.37E-05 2.73E-04 1.91E-05 6.31E-06 6.67E-06 2nd '16 14-Apr-16 4.08E-04 7.26E-06 5.42E-06 1.34E-03 2.16E-05 2.93E-05 1.69E-04 1.29E-05 5.76E-06 1.66E-05 2nd '16 14-Jun-16 5.92E-05 2.70E-06 4.00E-06 2.61E-04 2.09E-05 4.92E-05 2.10E-04 5.52E-06 1.70E-06 4.27E-06 4th '16 11-Nov-16 4.56E-05 2.10E-06 3.47E-06 2.70E-04 1.43E-05 3.81E-05 3.94E-05 5.94E-06 5.02E-06 2.10E-06 (5.00E-08) (l.OOE-06) (2.00E-07) •2nd quarter of 1996 San Juan County, Utah, was declared a d1saster area due to drought, no samples were collected dunng th1s penod t NRC Regulatory Guide does not specify a Lower Limit of Detection (LLD) for Thorium 232 in vegetation (or any matrix). The LLD for Thorium 230 was used. NS =Not Sampled NA =Not Applicable Th-232 MDC¥ ERROR LLD (uCi/Kg) uCi/Kg (2.0E-07)t NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 3.06E-06 4.04E-07 2.67E-06 6.78E-07 7.98E-07 7.06E-07 1.28E-06 7.67E-07 8.10E-07 9.31E-07 5.45E-07 5.66E-07 (2.00E-07) ¥The value in the MDC column is the sample-specific minimum detectable concentration. The MDC is based on the sample moisture, composition and other sample-specific variables. The value in parantheses is the method-specific lower limit of detection (LLD), which is a limit representing the detection capability of the measurement system. The LLDs in the data package are referred to as the Reporting limit (RL). (Log Scale) ...... ...... ...... ...... 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 CXl ....... (J) ()1 ~ w 1\:) 01-Aug-81 :e 01-Jun-82 ::::1: 01-Apr-83 =i 01-Feb-84 m 01-Dec-84 3: m 01-0ct-85 U) )> 01-Aug-86 -3: 01-Jun-87 • F 01-Apr-88 r- I 01-Feb-89 z 01-Dec-89 0 ::1:1 01-0ct-90 -4 t ::::1: 01-Aug-91 m 01-Jun-92 )> :Il U) ~ 01-Apr-93 -4 "' 1\) 0 0) 01-Feb-94 -., T 01-Dec-94 3: -01-0ct-95 r- -u r- 0" 01-Aug-96 ::1:1 ~ 01-Jun-97 DJ 0 c. f 01-Apr-98 -s· :J 01-Feb-99 c::: n c 01-Dec-99 z a: > 01-0ct-00 CJ -t 01-Aug-01 0 f 0 01-Jun-02 :J n -t 01-Apr-03 CJ I :J "' 01-Feb-04 -... c.> DJ 1\) 01-Dec-04 -s· 01-0ct-05 :J tn 01-Aug-06 :r 01-Jun-07 < 01-Apr-08 CJ CQ 01-Feb-09 -CJ -DJ 01-Dec-09 -s· 01-0ct-10 :J -01-Aug-11 c::: 01-Jun-12 0 :::::: 01-Apr-13 ;::llii CQ -01-Feb-14 01-Dec-14 01-0ct-15 01-Aug-16 WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHWEST OF MILL SAMPLED SAMPLED Ra-226 QTR. DATE VALUE (uCi/Kg) 3rd '81 27-Aug-81 2.73E-03 4th '81 20-0ct-81 2.00E-04 2nd '82 15-Apr-82 1.04E-04 3rd '82 01-Jul-82 2.00E-05 4th '82 30-Nov-82 2.36E-06 2nd '83 13-Apr-83 8.58E-05 3rd '83 01-Jul-83 1.19E-04 4th '83 30-Jan-84 9.78E-05 2nd '84 28-Jun-84 2.08E-04 4th '84 14-Nov-84 6.05E-04 2nd '85 27-Mar-85 l.IOE-04 3rd '85 15-Jul-85 6.JOE-05 4th '85 09-0ct-85 1.07E-04 2nd '86 24-Mar-86 8.86E-04 3rd '86 10-Jul-86 6.66E-04 4th '86 18-Dec-86 5.20E-04 2nd '87 20-Apr-87 4.JOE-04 3rd '87 05-Jun-87 1.60E-04 4th '87 22-Dec-87 3.60E-04 2nd '88 19-Apr-88 2.60E-04 3rd '88 28-Jul-88 3.10E-05 2nd '89 07-Apr-89 6.20E-04 3rd '89 06-Jun-89 3.40E-04 4th '89 07-Nov-89 5.10E-04 1st '90 17-Apr-90 3.60E-04 2nd '90 20-Jun-90 1.70E-04 3rd '90 17-0ct-90 8.80E-05 1st '91 10-Apr-91 3.00E-04 2nd'91 11-Jun-91 3.10E-04 3rd '91 20-Nov-91 5.00E-04 1st '92 22-Apr-92 2.00E-05 2nd '92 10-Jun-92 6.50E-06 3rd '92 10-Jun-92 1.20E-04 1st '93 13-Apr-93 1.80E-05 2nd '93 26-Jun-93 5.20E-05 3rd '93 12-0ct-93 5.10E-05 1st '94 I 1-May-94 1.20E-04 2nd '94 19-Jul-94 3.73E-05 3rd '94 28-Nov-94 2.40E-04 1st '95 I 1-Apr-95 8.40E-05 2nd '95 06-Jul-95 1.90E-05 3rd '95 15-Nov-95 l.20E-04 1st '96 23-Apr-96 8.30E-05 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 3.60E-05 1st '97 21-Apr-97 3.30E-05 3rd '97 05-Sep-97 5.40E-06 4th '97 20-Nov-97 8.90E-06 1st '98 23-Mar-98 <9.20E-05 2nd '98 16-Jun-98 < 6.50E-08 4th '98 05-Nov-98 4.20E-05 2nd '99 15-Apr-99 6.20E-05 3rd '99 07-Jul-99 5.45E-05 4th '99 02-Dec-99 l.IOE-04 2nd '00 21-Apr-00 3.70E-05 2nd '00 22-Jun-00 2.90E-05 4th '00 21-Dec-00 2.30E-06 1st 'OJ 30-Apr-01 2.10E-05 2nd '01 14-Jun-01 1.30E-06 4th '01 17-Dec-01 3.70E-05 1st '02 07-May-02 4.90E-05 2nd '02 07-Jul-02 8.88E-05 Ra-226 MDC¥ Pb-210 ERROR LLD uCi/Kg VALUE (uCi/Kg) (S.OE-08) (uCi/Kg) 5.00E-05 5.00E-08 7.JOE-03 J.OOE-05 5.00E-08 8.30E-04 9.00E-06 7.00E-06 6.40E-04 l.OOE-05 5.00E-08 2.20E-04 9.50E-07 l.OOE-06 8.00E-05 1.36E-05 2.00E-08 3.53E-04 l.IOE-05 5.00E-06 1.58E-04 7.00E-06 2.00E-06 2.16E-03 I.OOE-05 3.00E-09 1.60E-03 1.64E-04 2.00E-07 2.58E-03 8.00E-06 3.00E-06 8.63E-04 6.00E-06 2.00E-06 5.40E-04 6.00E-06 2.00E-06 3.80E-04 1.80E-05 2.00E-06 4.40E-03 1.80E-05 3.00E-06 4.78E-03 l.OOE-04 3.00E-06 1.70E-03 l.OOE-04 5.00E-08 1.60E-03 3.00E-05 5.00E-08 5.50E-04 5.00E-05 5.00E-08 1.80E-03 5.00E-05 5.00E-08 1.90E-03 1.90E-05 5.00E-08 1.60E-04 5.00E-05 *** 1.70E-03 3.00E-05 *** 7.40E-04 6.00E-05 7.00E-06 l.OOE-03 3.00E-05 4.00E-06 4.80E-04 2.00E-05 5.00E-08 3.20E-04 l.60E-05 5.00E-08 2.90E-04 3.00E-05 5.00E-06 4.10E-04 3.00E-05 2.00E-07 4.70E-04 4.00E-05 5.00E-08 1.50E-03 8.00E-06 2.00E-06 9.60E-05 6.00E-06 2.00E-06 1.20E-04 4.00E-05 3.00E-06 1.21E-03 1.70E-05 3.00E-06 2.JOE-04 1.90E-05 3.00E-06 1.70E-05 2.30E-05 3.00E-06 7.10E-04 l.OOE-05 3.00E-05 9.80E-04 1.60E-06 8.40E-08 7.80E-05 1.50E-05 1.70E-07 2.60E-04 6.LOE-06 1.50E-07 1.20E-04 1.50E-06 l.40E-07 4.50E-05 6.80E-06 1.40E-07 l.OOE-05 3.30E-06 l.90E-07 6.80E-05 2.50E-06 !.60E-07 8.50E-05 2.30E-06 l.70E-07 4.40E-05 3.50E-07 1.56E-07 3.20E-05 7.20E-07 5.40E-07 3.40E-04 9.20E-05 9.20E-05 <4.60E-04 6.50E-08 6.50E-08 <3.20E-07 l.OOE-06 l.IOE-07 l.70E-04 I.OOE-06 l.OOE-07 1.40E-04 1.40E-06 8.30E-08 9.20E-05 3.00E-06 2.20E-07 2.80E-05 l.OOE-06 2.40E-07 2.70E-04 l.OOE-06 3.30E-07 2.80E-04 1.40E-06 3.70E-07 3.30E-04 J.OOE-06 l.50E-07 <7.6E-07 4.00E-08 1.20E-07 1.80E-06 7.67E-07 8.30E-08 6.72E-05 2.40E-06 7.60E-07 1.28E-04 4.32E-06 7.60E-07 8.33E-05 Pb-210 MDC¥ U-NAT U-NAT MDC¥ Th-232 Th-232 MDC¥ ERROR LLD uCi/Kg VALUE ERROR LLD VALUE ERROR LLD (uCi/Kg) (l.OE-06) (uCi/Kg) (uCi/Kg) uCi/Kg (uCi/Kg) (uCi/Kg) uCi/Kg (2.0E-07) (2.0E-07)t 3.00E-04 l.OOE-06 NS NA NA NS NA NA 5.00E-05 J.OOE-06 NS NA NA NS NA NA 5.00E-05 4.00E-05 NS NA NA NS NA NA 9.00E-05 l.OOE-07 NS NA NA NS NA NA l.OOE-05 l.OOE-05 NS NA NA NS NA NA 1.90E-05 l.OOE-05 NS NA NA NS NA NA 1.30E-05 I.OOE-05 NS NA NA NS NA NA 3.40E-04 3.00E-04 NS NA NA NS NA NA 7.00E-05 3.00E-08 NS NA NA NS NA NA l.IOE-04 3.00E-08 NS NA NA NS NA NA 4.20E-05 3.00E-05 NS NA NA NS NA NA 5.00E-05 5.00E-05 NS NA NA NS NA NA 3.00E-05 2.00E-05 NS NA NA NS NA NA 1.90E-04 3.00E-05 NS NA NA NS NA NA 2.10E-04 6.00E-05 NS NA NA NS NA NA I.OOE-04 6.00E-05 NS NA NA NS NA NA l.OOE-04 I.OOE-06 NS NA NA NS NA NA 4.00E-05 l .OOE-06 NS NA NA NS NA NA I.OOE-04 l .OOE-06 NS NA NA NS NA NA l.OOE-04 I.OOE-06 NS NA NA NS NA NA 4.00E-05 l.OOE-06 NS NA NA NS NA NA l.OOE-04 *** NS NA NA NS NA NA 3.00E-05 *** NS NA NA NS NA NA 7.00E-05 1.40E-05 NS NA NA NS NA NA 2.00E-05 2.20E-05 NS NA NA NS NA NA 2.00E-05 l.OOE-06 NS NA NA NS NA NA 2.00E-05 l.OOE-06 NS NA NA NS NA NA 2.00E-05 l.OOE-06 NS NA NA NS NA NA 2.00E-05 2.00E-07 NS NA NA NS NA NA l.OOE-04 l.OOE-06 NS NA NA NS NA NA 1.40E-05 l.OOE-05 NS NA NA NS NA NA 2.00E-05 I.OOE-06 NS NA NA NS NA NA 8.00E-05 2.00E-05 NS NA NA NS NA NA 3.00E-05 2.00E-05 NS NA NA NS NA NA 3.60E-05 2.00E-05 NS NA NA NS NA NA 6.00E-05 2.00E-05 NS NA NA NS NA NA 1.60E-04 2.00E-04 NS NA NA NS NA NA 7.10E-06 4.20E-07 NS NA NA NS NA NA 1.30E-05 8.30E-07 NS NA NA NS NA NA l.IOE-05 7.50E-05 NS NA NA NS NA NA 4.30E-06 7.20E-07 NS NA NA NS NA NA 5.80E-06 7.10E-07 NS NA NA NS NA NA 6.30E-06 1.80E-07 NS NA NA NS NA NA NS NA NA NS NA NA 5.60E-06 8.40E-07 NS NA NA NS NA NA 4.80E-06 8.40E-07 NS NA NA NS NA NA 9.00E-07 7.83E-07 NS NA NA NS NA NA 6.70E-06 l.IOE-07 NS NA NA NS NA NA 4.60E-04 4.60E-04 NS NA NA NS NA NA 3.20E-07 3.20E-07 NS NA NA NS NA NA l.OOE-05 5.50E-07 NS NA NA NS NA NA 7.00E-06 l.OOE-07 NS NA NA NS NA NA 4.00E-06 4.20E-07 NS NA NA NS NA NA I.OOE-06 I.IOE-06 NS NA NA NS NA NA l.OOE-05 1.20E-06 NS NA NA NS NA NA 2.00E-05 1.70E-06 NS NA NA NS NA NA 5.00E-05 l.90E-06 NS NA NA NS NA NA NIA 7.60E-07 NS NA NA NS NA NA 3.00E-08 5.90E-07 NS NA NA NS NA NA 2.62E-06 6.00E-07 NS NA NA NS NA NA 5.61E-06 l.OOE-05 NS NA NA NS NA NA 4.32E-06 l.OOE-05 NS NA NA NS NA NA WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHWEST OF MILL SAMPLED SAMPLED Ra-226 QTR. DATE VALUE (uCi!Kg) 4th '02 15-Dec-02 1.50E-04 1st '03 21-Mar-03 5.00E-05 2nd '03 10-Jun-03 5.60E-05 4th '03 20-Nov-03 3.20E-04 1st '04 08-Apr-04 6.29E-05 2nd '04 12-Jun-04 6.51E-05 4th '04 30-Nov-04 7.50E-05 1st '05 21-Apr-05 4.90E-05 2nd '05 13-Jun-05 2.30E-05 4th '05 10-Nov-05 7.40E-05 1st '06 03-Apr-06 l.OOE-04 2nd '06 16-Jun-06 9.50E-05 4th '06 28-Nov-06 8.13E-05 1st '07 30-Mar-07 4.30E-05 2nd '07 1-Jun-07 5.10E-05 4th '07 23-Nov-07 7.30E-05 1st '08 22-Apr-08 2.80E-06 2nd '08 18-Jun-08 3.20E-06 4th '08 12-Dec-08 7.30E-05 1st '09 28-Apr-09 5.25E-05 2nd '09 17-Jun-09 2.30E-05 4th '09 18-Dec-09 5.50E-05 1st '10 13-May-10 1.90E-04 2nd '10 18-Jun-10 2.30E-05 4th '10 20-Dec-10 8.60E-06 2nd '11 23-Jun-11 2.10E-07 3rd '11 28-Ju1-11 4.20E-06 4th '11 23-Nov-11 7.70E-06 2nd '12 11-Apr-12 1.50E-05 3rd '12 11-Jun-12 8.30E-06 4th '12 06-Nov-12 2.34E-05 2nd'13 30-Apr-13 9.04E-05 3rd '13 20-Jun-13 2.58E-06 4th '13 14-Nov-13 1.43E-04 2nd '14 16-Apr-14 2.53E-05 3rd '14 10-Jun-14 2.53E-05 4th '14 25-Nov-14 7.41E-05 1st '15 21-Apr-15 1.31E-04 2nd '15 15-Jun-15 2.39E-04 4th '15 23-Nov-15 1.03E-04 2nd '16 14-Apr-16 1.28E-04 2nd '16 14-Jun-16 5.91E-05 4th '16 11-Nov-16 2.66E-04 Ra-226 ERROR (uCi!Kg) 6.20E-06 3.40E-06 2.00E-06 8.20E-06 4.10E-06 3.40E-06 4.60E-06 2.70E-06 2.10E-06 3.50E-06 6.00E-06 5.90E-06 4.10E-06 2.60E-06 3.20E-06 6.60E-06 2.80E-06 3.30E-06 3.20E-06 3.60E-06 1.60E-05 3.50E-06 6.10E-06 2.00E-06 9.10E-07 1.20E-07 5.40E-07 6.80E-07 9.50E-07 5.40E-07 4.10E-07 1.68E-06 9.59E-07 3.70E-06 6.29E-07 5.55E-07 1.90E-06 4.21E-06 4.43E-06 3.95E-06 4.20E-06 3.97E-06 4.22E-06 MDC¥ Pb-210 Pb-210 MDC¥ U-NAT U-NAT LLD uCi!Kg VALUE ERROR LLDuCi!Kg VALUE ERROR (S.OE-08) (uCi!Kg) (uCi!Kg) (l.OE-06) (uCi!Kg) (uCi/Kg) 7.60E-07 3.16E-04 1.07E-05 l.OOE-05 NS NA 2.71E-06 <4.2e-6 4.20E-06 NS NA 4.10E-07 1.88E-04 5.14E-06 8.20E-08 NS NA 1.70E-07 4.89E-04 1.25E-05 8.30E-07 NS NA 2.00E-07 1.94E-05 4.00E-06 l.OOE-06 NS NA 1.30E-07 1.87E-05 3.90E-06 6.50E-07 NS NA 2.00E-08 4.45E-04 1.40E-05 3.00E-07 NS NA 1.30E-07 1.27E-04 4.80E-06 6.50E-07 NS NA 1.50E-07 4.70E-05 5.10E-06 7.60E-07 NS NA 1.20E-10 2.40E-06 8.10E-08 5.80E-10 NS NA 5.00E-08 6.54E-04 1.50E-05 l.OOE-06 NS NA 5.00E-08 4.48E-04 1.40E-05 1.00E-06 NS NA 2.20E-07 3.25E-04 1.12E-06 l.OOE-05 NS NA 1.70E-07 2.64E-04 7.20E-06 8.60E-07 NS NA 2.30E-07 5.30E-04 1.40E-06 1.20E-06 NS NA 5.00E-08 7.00E-04 2.20E-05 l.lOE-06 NS NA 7.20E-07 4.40E-04 2.00E-05 l.OOE-06 NS NA 1.80E-06 1.40E-04 3.30E-05 5.50E-05 NS NA 7.40E-07 4.40E-04 2.50E-05 3.20E-05 NS NA l.IOE-06 1.90E-04 1.50E-05 2.20E-05 NS NA 5.20E-07 4.30E-05 l.OOE-05 1.70E-05 NS NA 3.00E-04 l.lOE-05 NS NA 9.40E-07 5.10E-04 2.40E-05 3.10E-05 NS NA 7.70E-07 8.30E-05 1.80E-05 2.90E-05 NS NA 3.90E-07 l.IOE-07 6.80E-07 l.IOE-06 NS NA 1.40E-07 <2.2E-06 1.30E-06 2.20E-06 NS NA 2.70E-07 2.30E-04 2.50E-06 2.30E-06 NS NA 2.30E-07 <5.8E-08 3.40E-07 5.80E-07 NS NA 2.60E-07 <7.0E-07 6.00E-07 l.OOE-06 NS NA 1.20E-07 1.40E-04 8.30E-06 6.50E-06 NS NA 7.71E-08 4.59E-04 3.83E-06 6.18E-07 NS NA 8.58E-07 2.24E-04 4.46E-06 4.68E-06 NS NA 8.06E-07 1.06E-04 2.30E-06 3.28E-06 NS NA 2.17E-06 4.65E-04 l.l?E-05 1.80E-05 NS NA 5.51E-07 5.70E-05 2.21E-06 4.52E-06 NS NA 5.77E-07 7.68E-05 2.08E-06 3.66E-06 NS NA 1.53E-06 2.98E-04 6.48E-06 1.06E-05 NS NA 5.92E-06 6.33E-04 l.l?E-05 1.45E-05 3.35E-04 2.41E-05 3.45E-06 1.08E-03 2.02E-05 3.25E-05 5.24E-04 2.41E-05 4.25E-06 4.78E-04 1.06E-05 1.75E-05 1.51E-04 1.53E-05 5.79E-06 3.56E-04 1.14E-05 1.86E-05 6.33E-05 8.20E-06 6.94E-06 1.73E-04 2.02E-05 5.42E-05 3.15E-05 1.90E-06 2.03E-06 1.28E-03 2.57E-05 4.95E-05 4.33E-04 2.58E-05 (5.00E-08) (l.OOE-06) •2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected dunng this penod MDC¥ Th-232 LLD VALUE uCi!Kg (uCi!Kg) (2.0E-07) NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS l.l?E-05 7.35E-06 9.70E-06 2.38E-05 7.71E-06 2.30E-05 5.95E-06 1.66E-06 1.54E-06 2.95E-06 8.24E-06 3.87E-06 (2.00E-07) t NRC Regulatory Guide does not specify a Lower Limit of Detection (LLD) for Thorium 232 in vegetation (or any matrix). The LLD for Thorium 230 was used. NS =Not Sampled NA =Not Applicable Th-232 MDC¥ ERROR LLD (uCi!Kg) uCi!Kg (2.0E-07)t NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8.57E-07 7.82E-07 2.12E-06 7.36E-07 1.53E-06 4.23E-07 4.81E-07 5.40E-07 8.26E-07 1.47E-06 7.58E-07 1.03E-06 (2.00E-07) ¥The value in the MDC column is the sample-specific minimum detectable concentration. The MDC is based on the sample moisture, composition and other sample-specific variables. The value in parantheses is the method-specific lower limit of detection (LLD), which is a limit representing the detection capability of the measurement system. The LLDs in the data package are refered to as the Reporting limit (RL). (Log Scale) ...... ...... ...... ...... 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 CXl "'-! en (11 .j:>. c.u 1\) :e 01-Aug-81 :X: 01-Jun-82 =t 01-Apr-83 m 01-Feb-84 s:: m 01-Dec-84 CJ) 01-0ct-85 )> s:: 01-Aug-86 -r 01-Jun-87 r 01-Apr-88 z 01-Feb-89 0 ::rJ 01-Dec-89 """' t 01-0ct-90 :X: :e 01-Aug-91 -m :0 CJ) 'l' 01-Jun-92 """' 1\} 0 1\} 01-Apr-93 0> 01-Feb-94 ., 1 s:: 01-Dec-94 -r "'0 01-0ct-95 r 0'" ::rJ r\J 01-Aug-96 ~ D) 0 c. 01-Jun-97 c;· t 01-Apr-98 ::J 01-Feb-99 c c 2. z 01-Dec-99 -a: )> CD -i 01-0ct-00 0 f 01-Aug-01 0 ::J 01-Jun-02 (') -i CD I 01-Apr-03 ::J r\J -w 01-Feb-04 ... 1\} D) -01-Dec-04 c;· 01-0ct-05 ::J 0 01-Aug-06 -· ::I 01-Jun-07 < 01-Apr-08 CD cc 01-Feb-09 ! D) 01-Dec-09 -c;· 01-0ct-10 ::I -01-Aug-11 c 0 01-Jun-12 :::::.: 01-Apr-13 " cc 01-Feb-14 - 01-Dec-14 01-0ct-15 01-Aug-16 WHITE MESA MILL FORAGE RADIONUCLIDE DATA SOUTHWEST OF MILL SAMPLED SAMPLED Ra-226 QTR. DATE VALUE (uCi!Kg) 3rd '81 27-Aug-81 9.50E-04 4th '81 20-0ct-81 3.00E-05 2nd '82 15-Apr-82 1.37E-05 3rd '82 01-Jul-82 3.40E-04 4th '82 30-Nov-82 1.75E-05 2nd '83 13-Apr-83 7.13E-04 3rd '83 01-Ju1-83 5.39E-05 4th '83 30-Jan-84 6.40E-05 2nd '84 28-Jun-84 8.27E-05 4th '84 14-Nov-84 2.72E-04 2nd '85 27-Mar-85 4.73E-04 3rd '85 15-Ju1-85 6.60E-05 4th '85 09-0ct-85 2.83E-04 2nd '86 24-Mar-86 1.57E-04 3rd '86 10-Ju1-86 3.78E-04 4th '86 18-Dec-86 2.60E-04 2nd '87 20-Apr-87 4.10E-04 3rd '87 05-Jun-87 2.90E-04 4th '87 22-Dec-87 1.80E-04 2nd '88 19-Apr-88 2.30E-04 3rd '88 28-Ju1-88 1.50E-04 2nd '89 07-Apr-89 3.10E-04 3rd '89 06-Jun-89 1.30E-04 4th '89 07-Nov-89 4.30E-04 1st '90 17-Apr-90 2.50E-04 2nd '90 20-Jun-90 l.IOE-04 3rd '90 17-0ct-90 6.10E-05 1st '91 10-Apr-91 3.40E-05 2nd '91 11-Jun-91 8.00E-05 3rd '91 20-Nov-91 6.50E-05 1st '92 22-Apr-92 1.60E-05 2nd '92 10-Jun-92 1.90E-05 3rd '92 10-Jun-92 1.60E-05 1st '93 13-Apr-93 2.60E-05 2nd '93 26-Jun-93 3.00E-05 3rd '93 12-0ct-93 3.10E-05 1st '94 11-May-94 2.00E-05 2nd '94 19-Ju1-94 1.75E-05 3rd '94 28-Nov-94 l.OOE-04 1st '95 11-Apr-95 1.70E-05 2nd '95 06-Ju1-95 6.40E-06 3rd '95 15-Nov-95 2.30E-05 1st '96 23-Apr-96 4.20E-05 2nd '96 * 31-Ju1-96 3rd '96 14-Nov-96 2.10E-05 1st '97 21-Apr-97 5.50E-06 3rd '97 05-Sep-97 5.30E-06 4th '97 20-Nov-97 2.50E-05 1st '98 23-Mar-98 <7.90E-05 2nd '98 16-Jun-98 3.60E-07 4th '98 05-Nov-98 4.30E-05 2nd '99 15-Apr-99 2.40E-05 3rd '99 07-Jul-99 2.23E-05 4th '99 02-Dec-99 1.50E-04 2nd '00 21-Apr-00 l.OOE-04 2nd '00 22-Jun-00 1.30E-06 4th '00 21-Dec-00 1.20E-06 1st '01 30-Apr-01 1.80E-06 2nd '01 14-Jun-01 2.60E-06 4th '01 17-Dec-01 2.63E-06 1st '02 07-May-02 3.50E-05 2nd '02 07-Jul-02 4.02E-05 4th '02 15-Dec-02 8.10E-05 Ra-226 MDC¥ ERROR LLDuCi/Kg (uCi/Kg) (S.OE-08) 2.00E-05 5.00E-08 3.00E-06 5.00E-08 3.00E-06 3.00E-06 2.00E-05 5.00E-08 3.00E-06 2.00E-06 7.30E-05 9.00E-08 4.50E-06 2.00E-06 7.00E-06 4.00E-06 6.30E-06 3.00E-09 1.48E-04 2.00E-07 1.60E-07 3.00E-06 7.00E-06 4.00E-06 2.00E-05 7.00E-06 l.OOE-05 4.00E-06 l.OOE-05 2.00E-06 2.00E-05 2.00E-06 7.00E-05 5.00E-08 4.00E-05 5.00E-08 3.00E-05 5.00E-08 5.00E-05 5.00E-08 3.00E-05 5.00E-08 4.00E-05 *** 2.00E-05 *** 5.00E-05 1.40E-05 3.00E-05 5.00E-06 2.00E-05 5.00E-08 1.40E-05 5.00E-08 1.10E-05 5.00E-06 6.00E-06 2.00E-07 1.40E-05 5.00E-08 7.00E-06 2.00E-06 I.OOE-05 2.00E-07 1.80E-05 3.00E-06 2.00E-05 3.00E-06 1.40E-05 3.00E-06 1.60E-05 3.00E-06 5.00E-06 3.00E-05 1.70E-06 7.60E-08 9.00E-06 1.50E-07 1.50E-06 1.60E-07 6.00E-07 1.40E-07 2.20E-06 1.70E-07 2.20E-06 1.70E-07 2.00E-06 1.60E-07 4.20E-07 1.40E-07 3.20E-07 1.26E-07 9.50E-07 5.90E-07 7.90E-05 7.90E-05 1.40E-07 3.30E-08 l.OOE-06 7.60E-08 I.OOE-06 1.20E-07 8.60E-07 1.20E-07 3.00E-06 2.00E-07 2.00E-06 1.20E-07 l.OOE-07 2.40E-07 9.00E-07 2.40E-07 l.OOE-07 1.70E-07 2.00E-07 9.90E-08 4.60E-05 1.20E-07 2.20E-06 7.60E-07 2.34E-06 7.60E-07 3.90E-06 7.60E-07 Pb-210 Pb-210 MDC¥ U-NAT U-N AT MDC¥ Th-232 Th-232 MDC¥ VALUE ERROR LLDuCi/Kg VALUE ERROR LLD VALUE ERROR LLD (uCi!Kg) (uCi!Kg) (l.OE-06) (uCi!Kg) (uCi/Kg) uCi!Kg (uCi!Kg) (uCi/Kg) uCi/Kg (2.0E-07) (2.0E-07)t 1.50E-04 l.OOE-05 l.OOE-06 NS NA NA NS NA NA 1.50E-04 2.00E-05 l.OOE-06 NS NA NA NS NA NA 3.80E-04 4.00E-05 4.00E-05 NS NA NA NS NA NA 3.68E-03 2.70E-04 l.OOE-07 NS NA NA NS NA NA 7.92E-04 4.00E-06 2.00E-05 NS NA NA NS NA NA 2.51E-03 3.00E-04 3.00E-04 NS NA NA NS NA NA 6.88E-04 4.30E-05 4.00E-05 NS NA NA NS NA NA 1.20E-03 l.OOE-04 4.00E-05 NS NA NA NS NA NA 1.80E-03 l.OOE-04 9.00E-08 NS NA NA NS NA NA 4.70E-03 7.20E-04 3.00E-07 NS NA NA NS NA NA 7.07E-04 3.60E-05 3.00E-05 NS NA NA NS NA NA 4.90E-04 3.00E-05 3.00E-05 NS NA NA NS NA NA l.SOE-03 l.OOE-04 7.00E-05 NS NA NA NS NA NA 4.14E-03 1.80E-04 3.00E-05 NS NA NA NS NA NA 1.65E-02 7.00E-04 1.00E-04 NS NA NA NS NA NA 1.70E-03 l.OOE-04 1.00E-04 NS NA NA NS NA NA 2.20E-03 1.00E-04 l.OOE-06 NS NA NA NS NA NA 7.50E-04 5.00E-05 l.OOE-06 NS NA NA NS NA NA 2.40E-03 l.OOE-04 l.OOE-06 NS NA NA NS NA NA 2.90E-03 l.OOE-04 l.OOE-06 NS NA NA NS NA NA 4.30E-03 2.00E-04 l.OOE-06 NS NA NA NS NA NA 4.20E-03 l.OOE-04 *** NS NA NA NS NA NA l.SOE-03 l.OOE-04 *** NS NA NA NS NA NA 3.50E-03 1.40E-04 2.70E-05 NS NA NA NS NA NA 2.39E-03 5.00E-05 2.50E-05 NS NA NA NS NA NA 6.60E-04 3.00E-05 l.OOE-06 NS NA NA NS NA NA 6.10E-04 3.00E-05 l.OOE-06 NS NA NA NS NA NA 2.20E-04 l.OOE-05 1.00E-06 NS NA NA NS NA NA 1.20E-04 l.OOE-05 2.00E-07 NS NA NA NS NA NA 9.10E-04 5.00E-05 l.OOE-06 NS NA NA NS NA NA 3.20E-04 2.00E-05 l.OOE-05 NS NA NA NS NA NA 2.20E-04 2.00E-05 l.OOE-06 NS NA NA NS NA NA 7.60E-04 6.00E-05 2.00E-05 NS NA NA NS NA NA 3.40E-04 3.00E-05 2.00E-05 NS NA NA NS NA NA O.OOE+OO 3.00E-05 2.00E-05 NS NA NA NS NA NA 4.20E-04 6.00E-05 2.00E-05 NS NA NA NS NA NA 3.90E-04 8.00E-05 2.00E-04 NS NA NA NS NA NA 1.30E-04 7.80E-06 3.80E-07 NS NA NA NS NA NA 2.60E-04 1.20E-05 7.40E-07 NS NA NA NS NA NA 1.60E-04 1.50E-05 8.10E-07 NS NA NA NS NA NA 4.40E-05 4.20E-06 7.00E-07 NS NA NA NS NA NA 6.60E-05 9.60E-06 8.30E-07 NS NA NA NS NA NA l.OOE-04 6.70E-06 1.80E-07 NS NA NA NS NA NA NS NA NA NS NA NA 1.90E-04 7.30E-06 8.20E-07 NS NA NA NS NA NA 3.30E-05 3.90E-06 7.00E-07 NS NA NA NS NA NA 1.90E-05 6.90E-07 6.34E-07 NS NA NA NS NA NA 1.30E-04 4.70E-06 1.20E-07 NS NA NA NS NA NA <3.90E-04 3.90E-04 3.90E-04 NS NA NA NS NA NA <1.7E-07 1.70E-07 1.70E-07 NS NA NA NS NA NA 2.50E-04 l.OOE-05 3.80E-07 NS NA NA NS NA NA 1.70E-04 8.00E-06 6.20E-07 NS NA NA NS NA NA 2.30E-04 7.00E-06 5.90E-07 NS NA NA NS NA NA 1.70E-05 l.OOE-06 l.OOE-06 NS NA NA NS NA NA l.IOE-04 7.00E-06 6.10E-07 NS NA NA NS NA NA 2.00E-04 l.OOE-05 1.20E-06 NS NA NA NS NA NA 1.20E-04 3.00E-05 1.20E-06 NS NA NA NS NA NA <8.3E-07 N/A 8.30E-07 NS NA NA NS NA NA l.IOE-06 2.00E-08 5.00E-07 NS NA NA NS NA NA 9.40E-05 3.72E-06 6.00E-07 NS NA NA NS NA NA 1.36E-04 5.61E-06 l.OOE-05 NS NA NA NS NA NA 7.04E-05 4.11E-06 l.OOE-05 NS NA NA NS NA NA 2.87E-04 8.54E-06 l.OOE-05 NS NA NA NS NA NA WHITE MESA MILL FORAGE RADIONUCLIDE DATA SOUTHWEST OF MILL SAMPLED SAMPLED Ra-226 QTR. DATE VALUE (uCi!Kg) 1st '03 21-Mar-03 3.70E-05 2nd '03 10-Jun-03 1.30E-05 4th '03 20-Nov-03 1.60E-04 1st '04 08-Apr-04 1.40E-04 2nd '04 12-Jun-04 6.51E-05 4th '04 30-Nov-04 8.40E-05 1st '05 21-Apr-05 1.70E-05 2nd'05 13-Jun-05 1.50E-05 4th '05 10-Nov-05 3.80E-05 1st '06 03-Apr-06 l.OOE-04 2nd '06 16-Jun-06 3.40E-05 4th '06 28-Nov-06 7.31E-05 1st '07 30-Mar-07 3.00E-05 2nd '07 1-Jun-07 l.IOE-04 4th '07 23-Nov-07 5.60E-05 lsi '08 22-Apr-08 3.20E-05 2nd '08 18-Jun-08 1.25E-05 4th '08 12-Dec-08 9.20E-05 1st '09 28-Apr-09 2.60E-05 2nd '09 17-Jun-09 2.40E-05 4th '09 18-Dec-09 3.10E-05 lsi '10 13-May-10 2.00E-05 2nd '10 18-Jun-10 l.IOE-05 4th '10 20-Dec-10 6.70E-06 2nd '11 23-Jun-11 <1.7E-07 3rd 'II 27-Jul-11 1.60E-05 4th 'II 23-Nov-11 7.80E-07 2nd '12 11-Apr-12 S.OOE-06 3rd '12 11-Jun-12 1.90E-08 4th '12 06-Nov-12 1.49E-05 2nd '13 30-Apr-13 4.50E-05 3rd '13 20-Jun-13 l.SlE-05 4th '13 14-Nov-13 1.18E-04 2nd '14 16-Apr-14 4.65E-05 3rd '14 10-Jun-14 1.23E-05 4th '14 25-Nov-14 1.16E-04 1st '15 21-Apr-15 2.27E-04 2nd '15 15-Jun-15 3.90E-05 4th '15 23-Nov-15 1.83E-04 2nd '16 14-Apr-16 1.67E-04 2nd '16 14-Jun-16 2.90E-05 4th '16 11-Nov-16 8.39E-05 Ra-226 MDC¥ ERROR LLDuCi!Kg (uCi!Kg) (S.OE-08) 2.60E-06 2.41E-06 I.OOE-06 5.20E-07 1.30E-05 1.20E-07 7.70E-06 l.IOE-07 3.20E-06 1.50E-07 5.70E-06 3.00E-08 1.60E-06 1.30E-07 1.60E-06 1.40E-07 2.10E-06 8.60E-10 6.00E-06 5.00E-08 2.50E-06 5.00E-08 3.20E-06 1.60E-07 2.20E-06 1.70E-07 4.60E-06 2.3-07 5.20E-06 5.00E-08 2.30E-06 7.20E-07 2.20E-06 1.80E-06 4.10E-06 9.60E-07 2.90E-06 1.40E-06 1.40E-06 3.90E-07 2.30E-06 2.10E-06 9.40E-07 1.30E-06 6.60E-07 9.10E-07 4.80E-07 6.90E-08 1.70E-07 l.OOE-06 2.60E-07 2.50E-07 2.30E-07 6.00E-07 3.00E-07 6.20E-08 l.IOE-07 3.4LE-07 4.25E-08 1.19E-06 5.39E-07 1.06E-06 1.96E-06 3.39E-06 2.97E-06 1.08E-06 7.35E-07 4.97E-07 6.97E-07 2.25E-06 1.53E-06 5.01E-06 4.08E-06 1.88E-06 2.71E-06 6.96E-06 9.64E-06 4.10E-06 3.65E-06 1.88E-06 3.85E-06 2.71E-06 3.21E-06 (5.00E-08) Pb-210 Pb-210 MDC¥ U-NAT U-NAT VALUE ERROR LLDuCi!Kg VALUE ERROR (uCi!Kg) (uCi/Kg) (l.OE-06) (uCi!Kg) (uCi/Kg) 2.69E-05 2.01E-06 3.73E-06 NS NA <l.OOE-07 l.OOE-07 NS NA 1.42E-04 6.42E-06 5.90E-07 NS NA 6.10E-06 2.70E-06 5.50E-07 NS NA 5.27E-05 4.90E-06 7.60E-07 NS NA 3.39E-04 1.60E-05 3.00E-07 NS NA 4.50E-05 3.50E-06 6.50E-07 NS NA 7.00E-05 5.JOE-06 6.90E-07 NS NA 1.20E-06 4.80E-08 4.30E-10 NS NA 3.30E-04 l.lOE-05 l.OOE-06 NS NA 1.37E-04 6.00E-06 l.OOE-06 NS NA 2.98E-04 8.50E-06 8.20E-07 NS NA 3.20E-04 7.90E-06 8.40E-07 NS NA 3.20E-04 l.lOE-05 I.IOE-06 NS NA 6.40E-04 1.90E-05 l.OOE-06 NS NA 2.30E-04 1.50E-05 I.OOE-06 NS NA 5.00E-05 3.00E-05 4.80E-03 NS NA 4.10E-04 3.00E-05 4.00E-05 NS NA 3.70E-05 1.50E-06 2.50E-05 NS NA 3.50E-05 7.90E-06 1.30E-05 NS NA 2.10E-04 8.40E-06 NS NA 5.60E-05 1.50E-05 2.40E-05 NS NA 7.80E-05 1.60E-05 2.50E-05 NS NA 8.00E-07 7.90E-07 1.30E-06 NS NA <2.5E-06 1.50E-06 2.50E-06 NS NA 9.50E-05 1.60E-06 l.?OE-06 NS NA <5.9E-07 3.50E-07 5.90E-07 NS NA <7.0E-07 7.00E-07 l.OOE-06 NS NA <2.5E-07 1.30E-06 2.20E-06 NS NA 4.45E-04 4.01E-06 8.57E-07 NS NA 3.62E-04 6.30E-06 9.90E-06 NS NA 6.71E-05 2.93E-06 6.24E-06 NS NA 5.92E-04 1.27E-05 1.62E-05 NS NA 2.13E-04 5.93E-06 1.31E-05 NS NA 2.46E-05 1.84E-06 4.63E-06 NS NA 4.43E-04 1.04E-05 1.94E-05 NS NA 5.90E-04 1.16E-05 1.67E-05 4.33E-04 1.86E-05 5.29E-04 1.61E-05 3.36E-05 7.78E-05 8.47E-06 8.94E-04 1.43E-05 2.03E-05 4.88E-04 2.91E-05 7.99E-04 2.08E-05 4.12E-05 2.10E-04 2.24E-05 1.95E-04 2.18E-05 5.93E-05 7.04E-05 3.17E-06 1.21E-03 2.15E-05 3.78E-05 1.27E-03 4.84E-05 (l.OOE-06) *2nd quarter of 1996 San Juan County, Utah, was declared a d1saster area due to drought, no samples were collected dunng th1s penod MDC¥ Th-232 LLD VALUE uCi/Kg (uCi!Kg) (2.0E-07) NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS NA NS 5.14E-06 3.31E-05 6.43E-06 1.08E-05 9.00E-06 7.92E-06 1.39E-05 5.58E-05 1.92E-06 3.70E-06 l.lOE-05 7.71E-06 (2.00E-07) t NRC Regulatory Guide does not specify a Lower Limit of Detection (LLD) for Thorium 232 in vegetation (or any matrix). The LLD for Thorium 230 was used. NS =Not Sampled NA =Not Applicable Th-232 MDC¥ ERROR LLD (uCi/Kg) uCi/Kg (2.0E-07)t NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2.15E-06 1.14E-06 1.28E-06 1.21E-06 7.67E-07 3.20E-07 5.42E-06 2.10E-06 8.08E-07 1.04E-06 1.08E-06 1.32E-06 (2.00E-07) ¥The value in the MDC column is the sample-specific minimum detectable concentration. The MDC is based on the sample moisture, composition and other sample-specific variables. The value in parantheses is the method-specific lower limit of detection (LLD), which is a limit representing the detection capability of the measurement system. The LLDs in the data package are refered to as the Reporting limit (RL). (Log Scale) _. -- ----0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m m m I I I 6 I I I I + 0 0 0 0 0 0 0 0 (X) ....... O'l 01 """ UJ 1\) _. 0 01-Aug-81 :e ::::r:: 01-Jun-82 =i 01-Apr-83 m 01-Feb-84 3: m 01-Dec-84 en )> 01-0ct-85 3: 01-Aug-86 -r 01-Jun-87 r I 01-Apr-88 en 01-Feb-89 0 c: 01-Dec-89 -t t 01-0ct-90 ::::r:: :e 01-Aug-91 m JJ en I!' 01-Jun-92 -t 1\) 1\) 01-Apr-93 0 0> 01-Feb-94 ., T 3: 01-Dec-94 -r "'0 01-0ct-95 r c:r r\J 01-Aug-96 J] ~ Q) 0 a. 01-Jun-97 s· t 01-Apr-98 ::::s 01-Feb-99 c c n z 01-Dec-99 c: )> -1 01-0ct-00 (D 0 t 01-Aug-01 0 ::::s 01-Jun-02 n -1 (D I 01-Apr-03 ::::s r\J ... C.J 01-Feb-04 .., 1\) m ... 01-Dec-04 s· 01-0ct-05 ::::s tn 01-Aug-06 ::::s 01-Jun-07 < (D 01-Apr-08 (Q (D 01-Feb-09 ... m 01-Dec-09 ... s· 01-0ct-10 ::::s -01-Aug-11 c 0 01-Jun-12 =:::.: 01-Apr-13 ~ (Q -01-Feb-14 01-Dec-14 01-0ct-15 · 01-Aug-16 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171-www.gel.com Certificate of Analysis Report Date: December 29,2016 Company: Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Vegetation Analysis ------------------------------North East 410794001 Vegetation 11-NOV-16 08:30 17-NOV-16 Client Project: Client ID: DNMIOOIOI DNMI001 ----- Parameter Qualifier Result Uncertainty ~ad Alpha Spec Analysis \lphaspec Th-232, Solid "Dry Weight Corrected" ~horium-232 2. I OE-06 +/-5.45E-07 \lphaspec U, Solid "Dry Weight Corrected" Jranium-233/234 1.66E-05 +/-2.43E-06 Jranium-235/236 U 8.50E-07 +/-7.38E-07 Jranium-238 2.19E-05 +/-2. 77E-06 ~ad Gas Flow Proportional Counting :JFPC, Pb210, Solid "Dry Weight Corrected" ,ead-210 0.00027 +/-1.43E-05 :JFPC, Total Alpha Radium, solid "Dry Weight Corrected" ~otal Radium 4.56E-05 +/-2.1 OE-06 rhe following Prep Methods were performed: \1ethod Description )ry oil Prep Dry 'oil Prep GL-RAD-A-021 The following Analytical Methods were performed: \1etbod Descri tion DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified EPA 900.1 Modified Test MDC RL 5.66E-07 2.00E-07 2.13E-06 2.00E-07 1.27E-06 2.00E-07 1.62E-06 2.00E-07 3.81E-05 l.OOE-06 3.47E-06 5.00E-08 Analyst JX01 Units PF DF Analyst Date uCi/kg HAKB 12/14/16 uCi/kg HAKB 12/15/16 uCi/kg uCi/kg uCi/kg KSDI 12/28/16 uCi/kg KSDI 12/15/16 Date Time Prep Batch 11/18/16 1454 1617917 Anal st Comments Result Nominal Recovery% )urrogate/Tracer Recovery [horium-229 Tracer Jranium-232 Tracer ------------------ ,ead Carrier 3arium Carrier ~otes: Alphaspec Th-232, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" GFPC, Total Alpha Radium, solid "Dry Weight Corrected" =:ounting Uncertainty is calculated at the 68% confidence level (1-sigma). 92.5 98.7 83.8 94.1 Time Batch Method 1344 1620043 1541 1620044 0917 1625688 2005 1619907 ----- Acceptable Limits (15%-125%) (15%-125%) (25%-125%) (25%-125%) 2 3 4 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 29,2016 Company: Address: Contact: Project: Client Sample ID: Sample ID: Parameter Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Vegetation Analysis North East 410794001 MDC RL Qualifier Result Uncertainty ----------------~-------------~--------------- Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Lc/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Project: Client ID: DNMIOOlOl DNMIOOl Units PF DF Analyst Date Time Batch Method GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171-www .gel.com Certificate of Analysis Report Date: December 29,2016 Company: Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Vegetation Analysis North West 410794002 Vegetation 11-NOV-16 09:30 17-NOV-16 Client MDC RL Parameter Qualifier Result Uncertainty ----~------------------~ad Alpha Spec Analysis \lphaspec Th-232, Solid "Dry Weight Corrected" ~horium-232 3.87£-06 +/-7 .58£-07 \lphaspec U, Solid "Dry Weight Corrected" Jranium-233/234 0.000214 +/-1.12£-05 Jranium-235/236 2.08E-05 +/-3.93E-06 Jranium-238 0.000198 +/-1.07E-05 ~ad Gas Flow Proportional Counting }FPC, Pb210, Solid "Dry Weight Corrected" "ead-210 0.00128 +/-2.57E-05 }FPC, Total Alpha Radium, solid "Dry Weight Corrected" ~otal Radium 0.000266 +/-4.22E-06 [he following Pre Methods were erformed: 1.03E-06 2.00E-07 3.14E-06 2.00E-07 2.15E-06 2.00E-07 2.95E-06 200£-07 4.95£-05 l.OOE-06 2.03£-06 5.00E-08 Vlethod Description )ry Soil Prep --;c;D:-ry-,S""o""'ii;-;P,-re-p-:G:;-;L--""RA~D--A:--~02~1:----------------=;;c-;-"'--Analyst JX01 The following Analytical Methods were performed: \1ethod -~D~e~s~c~ri~p~ti~on~----~----~~~-------------------- DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified EPA 900.1 Modified Project: Client ID: DNMI00101 DNMI001 Units PF DF Analyst Date Time Batch Method uCi/kg HAKB 12/14/16 1332 1620043 uCi/kg HAKB 12/15/16 1232 1620044 2 uCilkg uCi/kg uCilkg KSD1 12/28/16 0917 1625688 3 uCi/kg KSD1 12115/16 2005 1619907 4 Date Time Prep Batch 11/18/16 1454 1617917 Analyst Comments )urrogate/Tracer Recovery rhorium-229 Tracer Jranium-232 Tracer Test Result Nominal Recovery% 86.4 60.3 63.1 104 Acceptable Limits (15%-125%) (15%-125%) (25%-125%) (25%-125%) "ead Carrier 3arium Carrier ~otes: Alphaspec Th-232, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" GFPC, Total Alpha Radium, solid "Dry Weight Corrected" :ounting Uncertainty is calculated at the 68% confidence level (1-sigma). GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171-www.gel.com Certificate of Analysis Report Date: December 29,2016 Company: Address: Contact: Project: Client Sample ID: Sample ID: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Vegetation Analysis North West 410794002 Parameter Qualifier Result Uncertainty MDC Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Lc/LC: Critical Level PF: Prep Factor RL: Reporting Limit RL MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Project: Client ID: DNMIOOlOl DNMIOOl Units PF DF Analyst Date Time Batch Method GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 29,2016 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: Vegetation Analysis ----------~------------~---------------------------------Client Sample ID: South West Sample ID: 410794003 Matrix: Vegetation Collect Date: 11-NOV-16 10:00 ReceiveDate: 17-NOV-16 Collector: Client Parameter Qualifier Result Uncertainty ~ad Alpha Spec Analysis \lphaspec Th-232, Solid "Dry Weight Corrected" ~horium-232 7.71E-06 +/-1.08E-06 \lphaspec U, Solid "Dry Weight Corrected" Jranium-233/234 0.000592 +/-2.08E-05 Jranium-235/236 3.69E-05 +/-5.85E-06 Jranium-238 0.000643 +/-2.17E-05 ~ad Gas Flow Proportional Counting :JFPC, Pb210, Solid "Dry Weight Corrected" ,ead-210 0.00121 +/-2.15E-05 :JFPC, Total Alpha Radium, solid "Dry Weight Corrected" ~otal Radium 8.39E-OS +/-2.71E-06 rhe following Prep Methods were performed: IJethod Description )ry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: \tlethod Descri2tion DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified EPA 900.1 Modified )urrogate/Tracer Recovery Test MDC 1.32E-06 3.72E-06 3.80E-06 3.44E-06 3.87E-05 3.21E-06 rhorium-229 Tracer Jranium-232 Tracer ,ead Carrier 3arium Carrier Alphaspec Th-232, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb21 0, Solid "Dry Weight Corrected" GFPC, Total Alpha Radium, solid "Dry Weight Corrected" "Jotes: RL 2.00E-07 2.00E-07 2.00E-07 2.00E-07 l.OOE-06 5.00E-08 Analyst JXOI =:ounting Uncertainty is calculated at the 68% confidence level (1-sigma). Project: Client ID: DNMIOOlOl DNMIOOl Units PF DF Analyst Date uCi/kg uCi/kg uCi/kg uCi/kg uCi/kg uCi/kg Date 11/18/16 Result HAKB 12/14/16 HAKB 12/15/16 KSDI 12/28/16 KSDI 12/15/16 Time Prep Batch 1454 1617917 Analys! Comments Nominal Recovery% 84.8 39.6 83.1 89.3 Time Batch Method 1332 1620043 1232 1620044 2 0917 1625688 3 2005 1619907 4 Acceptable Limits (15%-125%) (15%-125%) (25%-125%) (25%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171-www.gel.com Certificate of Analysis Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: Vegetation Analysis --~------------------------Client Sample ID: South West Sample ID: 410794003 Project: Client ID: Report Date: December 29,2016 DNMIOOIOI DNMIOOl Parameter Qualifier Result Uncertainty ----------------~------MDC RL Units PF DF Analyst Date Time Batch Method Column headers are defined as follows : DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Lc/LC: Critical Level PF: Prep Factor RL: Reporting Limit ------------------ SQL: Sample Quantitation Limit m ij •I Laboratories LLC a member of The GEL Group INC PO Box 30712 Charleston. SC 29417 2040 Sa•1age Road Charleston. SC 29407 p 843.556.8171 F 843.766.117B December 29,2016 Ms. Kathy Weinel Energy Fuels Resources (USA), lnc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: Vegetation Analysis Work0rder:410794 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on November 17,2016. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DW16138 Enclosures Sincerely, Julie Robinson Project Manager gel. co rn December 29,2016 Laborator·y Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 410794 Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on November 17, 2016 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Jdentification: The laboratory received the following samples: Laboratory ID Client ID 410794001 North East 410794002 North West 410794003 South West Case Narrative: Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Julie Robinson Project Manager Sheet 1 of 1 , CHAIN OF CUSTODY, Samples Shipped to: Gel Laboratories Contact: Garrin Palmer ~2-0~40~S-av~a~g~e~R~o~a-d~--------------Ph:4356782221 Charleston, SC 29407 gpalmer@energvtuels.com Chain of Custody/Sampling Analysis Request p . t roJec s amp1ers N a me ' s amp ers Sl 1gnature Late Fall Vegetation 2016 Garrin Palmer I / 6} L LJ·"~· ·-c/ ~- Time Sample 10 Date Collected Collected Laboratory Analysis Requested North East 11/11/201.6 830 Ra 226, U-Nat, Th-232, PB 210 North West 11/11/2016 ' 930 . Ra 226, U-Nat, Th-232, PB 210 South West 11/11/2016 1000 " Ra 226, U-Nat, Th-232·, PB 21 0 .. Weights: • I North East: 3945Grams < North West: 3380 Grams South West: 3830 Grams ~ * Please use caution when handling samples. Cactus · and Yucca plants are included the samples . . " .,. Comments: Please send report to Kathy Weinel at kweinel@energyfuels.com Relinquished ~y:(SiC-Date/Time Received By:(Signature) Date/Time Cz~~ · n/tt/j(. C!Jr..ro~. II }nh ~ YZ) I 'lJ6 . Relinquished By: (Signature) Date/Time Re~~ived By:·(Signature) Date/Time HI Laboratories LLC Received By: f\-(1 Suspected Hazard Information COC/Sam les marked as radioactive? Classified Radioactive II or III b RSO? COC/Samples marked containing PCBs? Package, COC; andlor:Samples marked as becyllium or,:isbeslos containiti' •? and tracking number. Comments (Use Continuation Fonn if needed): ~ SAMPLE RECEIPT & REVIEW FORM SDC/AR/COC/Woa·k Date Received: *If Net Counts> IOOcpm on samples not marked "radioactive", contact ~1c Radiation Safety Group for further investigation. Maximum Net Counts Observed* (Observed Counts-Area Back _ If yes, Were swipes taken of sample containers< action levels? If yes; samp)es are to be segregated as Safety ,Controlled Samples, and opened b Hazard Class Shipped: UN#: None Other (describe) - Damaged container Leaking conrnincr Other (describe) ID's, contajners affected ontl observed pH: FcdEx Air FcdEx Ground UPS Field Services Courier Otl1er - 1? 1<6·1 YLf y rt-1~1 ~4 v lt-1~7 Ylf y 6 3 q 1 ~c.t Lf( ? s~ ~u)o qs{:;s- '1 LfSLJ GL-CHL-SR-001 Rev 3 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 410794 Client SDG: 410794 Late Spring Vegetation 2016 Project Manager: Project Name: Purchase Order: Package Level: EDD Format: Julie Robinson DNMI00101 Vegetation Analysis DW16138 LEVEL3 EIM_DNMI Collect GELID Client Sample ID Client Sample Desc. Date & Time 410794001 North East 41 0794002 North West 410794003 South West Client Sample ID -001 North East -002 North West -003 South West Status Tests/Methods REVW Alphaspec Th-232, Solid REVW Alphaspec U, Solid 11-NOV-16 08:30 11-NOV-16 09:30 11-NOV-16 10:00 Product Reference U-Natural REVW GFPC, Total Alpha Radium, solid Ra226 REVW GFPC, Pb210, Solid REVW Laboratory Composite -Dry prep instructions REVW Alphaspec Th-232, Solid REVW Alphaspec U, Solid U-Natural REVW GFPC, Total Alpha Radium, solid Ra226 REVW GFPC, Pb210, Solid REVW Laboratory Composite -Dry prep Instructions REVW Alphaspec Th-232, Solid REVW Alphaspec U, Solid U-Natural REVW GFPC, Total Alpha Radium, solid Ra226 REVW GFPC, Pb210, Solid REVW Laboratory Composite -Dry prep instructions Work Order Due Date: Package Due Date: EDD Due Date: Due Date: HXT1 Receive Time #of 17-DEC-16 15-DEC-16 16-DEC-16 17-DEC-16 Lab Report Date: 29-DEC-16 Work Order: 410794 Page 1 of 3 Collector: C Prelogin #: 20160443172 Project Workdef ID: 1310529 SDG Status: Closed Logged by: Fax Days to Prelog Lab Field Date & Time Zone Cont. Matrix Due Date Process CofC# Group QC QC 17-NOV-16 09:25 -2 1 VEGETATION 17-NOV-16 09:25 -2 1 VEGETATION 17-NOV-16 09:25 -2 1 VEGETATION Fax Date PM Comments Please use caution when Cooler Seal Undisturbed handling samples. Cactus and Yucca plants are included in Temperature {C) samples Please use caution when Cooler Seal Undisturbed handling samples. Cactus and Yucca plants are included in Temperature (C) samples Please use caution when Cooler Seal Undisturbed handling samples. Cactus and Yucca plants are included in Temperature {C) samples 30 30 30 Aux Data y 18 y 18 y 18 Receive Codes GEL Laboratories LLC -Login Review Report Product: ASP_ THS Workdef ID: 1370540 In Product Group? No Method: DOE EML HASL -300, Th-01-RC Modified Product Description: Alphaspec Th-232, Solid Samples: 001, 002, 003 Parmname Check: All parmnames scheduled properly CAS# Parmname 7440-29-1 Thorium-232 Product: LABCOMP_S WorkdefiD: 1310628 Method: In Product Group? No Product Description: Laboratory Composite -Dry prep instructions Samples: 001, 002, 003 Parmname Check: All parmnames scheduled properly CAS# Parmname Product: GFC PBS Workdef ID: 1310600 In Product Group? No - Method: DOE RP280 Modified Product Description: GFPC, Pb210, Solid Samples: 001, 002, 003 Parmname Check: All parmnames scheduled properly CAS# Parmname 14255-04-0 Lead-210 Product: GFCTORAS WorkdefiD: 1310679 In Product Group? No Method: EPA 900.1 Modified Product Description: GFPC, Total Alpha Radium, solid Samples: 001, 002, 003 Parmname Check: All parmnames scheduled properly CAS# Parmname Total Radium Group Name: Client RDL or PQL & Unit .0000002 Group Name: Client RDL or PQL & Unit Group Name: Client RDL or PQL& Unit .000001 Group Name: Client RDL or PQL & Unit .00000005 Group Reference: Report Date: 29-DEC-16 Work Order: 410794 Page 2 of 3 Path: No Ash pCi/g Product Reference: Moisture Correction: "Dry Weight Corrected" Reporting Parm Included Included Custom Units Function in Sample? in QC? List? uCilkg Reporting Units Reporting Units uCi/kg Reporting Units uCi/kg REG y y Yes Group Reference: Path: Rad Prep SPRP Product Reference: Moisture Correction: "As Received" Parm Included Included Custom Function in Sample? in QC? List? No Group Reference: Path: Standard Product Reference: Moisture Correction: "Dry Weight Corrected" Parm Included Included Custom Function in Sample? inQC? List? REG y y Yes Group Reference: Path: Standard Product Reference: Ra226 Moisture Correction: "Dry Weight Corrected" Parm Included Included Custom Function in Sample? inQC? List? REG y y Yes GEL Laboratories LLC -Login Review Report Product: ASP _UUS Workdef ID: 1370669 In Product Group? No Method: DOE EML HASL -300, U-02-RC Modified Product Description: Alphaspec U, Solid Samples: 001, 002, 003 Parmname Check: All parmnames scheduled properly CAS# Parmname 13968-55-3/13966-Uranium-233/234 15117-96-1/13982-Uranium-235/236 7440-61-1 Uranium-238 Contingent Tests Action Product Name Login Requirements: Requirement Are these vegetation sample? Login Reminder? Description Group Name: Client RDL or PQL & Unit .0000002 .0000002 .0000002 Samples Group Reference: Path: Standard Report Date: 29-DEC-16 Work Order: 410794 Page 3 of 3 Product Reference: U-Natural Moisture Correction: "Dry Weight Corrected" Reporting Parm Included Included Custom Units Function in Sample? in QC? List? uCilkg uCilkg uCilkg REG REG REG y y y y y y Yes Include? Comments y y FOR VEGETATION: After logging in, change from DRY to WET in sample inquiry. FOR VEGETATION: After logging in, change from DRY to WET in sample inquiry. Log with lab camp. Peer Review by: ___________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? _____ _ Method/Analy. i Information Radiochemistry Technical Case Narrative Energy Fuels Resources (DNMI) SDG #: 410794 Product: Alphaspec Th-232, Solid Analytical Method: DOE EML HASL-300, Th-01-RC Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1620043 Prep Batch Number: 1617917 Sample ID 410794001 410794002 410794003 1203679886 1203679888 1203679887 Client ID North East North West South West Method Blank (MB) Laboratory Control Sample (LCS) 410794003(South West) Sample Duplicate (DUP) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-038 REV# 17. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control CQC) Information: Blank Information The blank volume is representative of the sample volumes in this batch. QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The sample and the duplicate, 1203679887 (South WestDUP) and 410794003 (South West), did not meet the Th-232 relative percent difference requirement; however, they do meet the relative error ratio requirement with a value of 1.02. The blank did not meet the Th-232 detection limit due to keeping the blank volume consistent with the other sample aliquots. All other samples met the detection limits. Designated QC The following sample was used for QC: 410794003 (South West). Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-p rep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Recounts Sample 1203679886 (MB) was recounted due to a suspected blank false positive. The recount is reported. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Manual Integration No manual integrations were performed on data in this batch. Sample-Specific MDA/MDC The MD A/MDC reported on the certificate of analysis is a sample-specific MD A/MDC. Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required. Method/Analysis Information Product: Alphaspec U, Solid Analytical Method: DOE EML HASL-300, U-02-RC Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1620044 Prep Batch Number: 1617917 Sample ID 410794001 410794002 410794003 1203679889 1203679891 1203679890 Client ID North East North West South West Method Blank (MB) Laboratory Control Sample (LCS) 410794002(North West) Sample Duplicate (DUP) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-011 REV# 26. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control <QC) Information: Blank Information The blank volume is representative of the sample volumes in this batch. QC Information All of the QC samples meet the required acceptance limits with the following exceptions: Refer to Miscellaneous Information section. The sample and the duplicate, 1203679890 (North WestDUP) and 410794002 (North West), did not meet the U-235/236 relative percent difference requirement; however, they do meet the relative error ratio requirement with a value of0.855. Designated QC The following sample was used for QC: 410794002 (North West). Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Recounts Batch was recounted in order to reduce tailing. The recounts are being reported. Miscellaneous Information: Data Exception (DER) Documentation A data exception report (DER) 1587772 was generated for samples 1203679889 (MB) and 410794001 (North East) in this SDG/batch. DER 1587772 was generated due to RDL less than MDA. I. Sample 410794001 did not meet the U-235/236 and the Method blank 1203679889 did not meet the U-233/234, U-235/236, and U-238 detection limits. I. Samples did not meet the detection limits due to reduced count times. The batch count times were reduced in order to minimize tailing from high levels of activity in the samples. The blank count time was reduced in order to keep consistent with the sample count times. Reporting results. Manual Integration No manual integrations were performed on data in this batch. Sample-Specific MDA/MDC The MD A/MDC reported on the certificate of analysis is a sample-specific MD A/MDC. Additional Comments Additional comments were not required for this sample set. OuaJificr Information Manual qualifiers were not required. Method/An alysis rnrormation Product: GFPC, Total Alpha Radium, solid Analytical Method: EPA 900.1 Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1619907 Prep Batch Number: 1617917 Sample ID 410794001 410794002 410794003 1203679533 1203679536 1203679534 1203679535 Client ID North East North West South West Method Blank (MB) Laboratory Control Sample (LCS) 410794003(South West) Sample Duplicate (DUP) 410794003(South West) Matrix Spike (MS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-010 REV# 15. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Conti"OI (OC) Information: Blank Information The blank volume is representative of the sample volume in this batch. QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The blank, 1203679533 (MB), did not meet the detection limit due to keeping the blank volume consistent with the other sample aliquots. All other samples met the detection limits. The sample and the duplicate, 1203679534 (South WestDUP) and 410794003 (South West), did not meet the relative percent difference requirement; however, they do meet the relative error ratio requirement with a value of2.36. Designated QC The following sample was used for QC: 410794003 (South West). Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep!Re-analysis None of the samples in this sample set required reprep or reanalysis. Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set. Recounts None of the samples in this sample set were recounted. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Sample-Specific MDA/MDC The MD A/MDC reported on the certificate of analysis is a sample-specific MD A/MDC. Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required. Method/ Analysis Information Product: GFPC, Pb210, Solid Analytical Method: DOE RP280 Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1625688 Prep Batch Number: 1617917 SampleiD 410794001 410794002 410794003 1203694009 1203694012 1203694010 1203694011 Client ID North East North West South West Method Blank (MB) Laboratory Control Sample (LCS) 410794002(North West) Sample Duplicate (DUP) 410794002(North West) Matrix Spike (MS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-018 REV# 13. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control (OC) Information: Blank Information The blank volume is representative of the sample volume in this batch. QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The blank, 1203694009 (MB), did not meet the detection limit due to keeping the blank volume consistent with the other sample aliquots. All other samples met the detection limits. Designated QC The following sample was used for QC: 410794002 (North West). Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis Samples were reprepped due to high relative percent difference/relative error ratio. The re-analysis is being reported. Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set. Recounts None of the samples in this sample set were recounted. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Sample-Specific MDAIMDC The MD A/MDC reported on the certificate of analysis is a sample-specific MD A/MDC. Additional Comments The matrix spike, 1203694011 (North WestMS), aliquot was reduced to conserve sample volume. OuaJifier Information Manual qualifiers were not required. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171-www.gel.com Qualifier Definition Report for DNMI001 Energy Fuels Resources (USA), Inc. Client SDG: 410794 GEL Work Order: 410794 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. Review/Validation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: Name: Kate Gellatly Date: 29 DEC 2016 Title: Analyst I GEL Laboratories LLC Form GEL-DER - DER Report No.: 1587772 Revision No.: 1 - DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: Type: 16-DEC-16 Radiochemistry Specifications Process Instrument Type: Test I Method: Matrix Type: Client Code: ALPHA SPECTROMETER DOE EML HASL-300, U-02-RC Solid DNMI Modified Batch ID: Sample Numbers: 1620044 See Below Potentially affected work order(s)(SDG):410794 Application Issues: RDL less than MDA Specification and Requirements DER Disposition: Exception Description: 1. Sample 410794001 did not meet the U-235/236 and the Method blank 1. Samples did not meet the detection limits due to reduced count times. 1203679889 did not meet the U-233/234, U-235/236, and U-238 The batch count times were reduced in order to minimize tailing from high detection limits. levels of activity in the samples. The blank count time was reduced in order to keep consistent with the sample count times. Reporting results. Originator's Name: Data Validator/Group Leader: Jessica Downey 16-DEC-16 Jessica Davis 16-DEC-16 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407-(843) 556-8171 -www.gel.com QC Summar.1: Reoort Date: December 29,2016 Energy Fuels Resources (USA), Inc. Page 1 of 225 Union Boulevard Suite 600 Lakewood, Colorado Contact: Ms. Kathy Weinel Workorder: 410794 Parmname NOM Sampk_9ual c Units RPD% REC% Ran e Anlst Date Time Rad Alpha Spec 3atch 1620043 QCI203679887 410794003 DUP Thorium-232 7.7IE-06 9.60E-06 uCi/kg 21.9* (0%-20%) HAKB 12/14116 13:1 Uncertainty +/-1.08E-06 +/-1.28E-06 QCI203679888 LCS Thorium-232 0.000131 0.000132 uCi/kg 101 (75%-125%) 12114116 13:3 Uncertainty +/-4.08E-06 QCI203679886 MB Thorium-232 u 7.36E-08 uCi/kg 12/15/16 15 :4 Uncertainty +/-3.62E-07 3atch 1620044 QC 1203679890 410794002 DUP Uranium-233/234 0.000214 0.000202 uCi/kg 5.8 (0%-20%) HAKB 12/15/16 12:1 Uncertainty +/-l.l2E-05 +/-9.22E-06 Uranium-235/236 2.08E-05 1.60E-05 uCi/kg 26.3* (0%-20%) Uncertainty +/-3.93E-06 +/-2.94E-06 Uranium-238 0.000198 0.000198 uCi/kg 0.0136 (0%-20%) Uncertainty +/-1.07E-05 +/-9.13E-06 QC1203679891 J,.CS Uranium-233/234 7.48E-05 uCi/kg 12/15/16 12:1 Uncertainty +/-5 .06E-06 Uranium-235/236 3.67E-06 uCi/kg Uncertainty +/-1 .33E-06 Uranium-238 6.71E-05 6.85E-05 uCilkg 102 (75%-125%) Uncertainty +/-4.84E-06 QCI203679889 MB Uranium-233/234 u 1.28E-06 uCi/kg 12/15/16 15:4 Uncertainty +/-7.39E-07 Uranium-23 5/236 u 2.81E-07 uCi/kg Uncertainty +/-5 .28E-07 Uranium-238 u 3.83E-07 uCi/kg Uncertainty +/-5.27E-07 Rad Gas Flow 3atch 1619907 QC1203679534 410794003 DUP Total Radium 8.39E-05 6.75E-05 uCi/kg 21.8* (0%-20%) KSD1 12/15/16 20:0 Uncertainty +/-2. 71E-06 +/-2.31E-06 QC 1203679536 LCS Total Radium 0.00395 0.00304 uCi/kg 76.9 (75%-125%) 12/15/1613:4 Uncertainty +/-4.59E-05 QC1203679533 MB Total Radium u -5.23E-08 uCi/kg 12/15/16 20:0 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407-(843) 556-8171-www.gel.com QC Summary Workorder: 410794 Parmname Rad Gas Flow --------------~NOM 3atch 1619907 Uncertainty QC1203679535 410794003 MS Total Radium 0.014 8.39E-05 Uncertainty +/-2.71E-06 3atch 1625688 QC1203694010 410794002 DUP Lead-210 0.00128 Uncertainty +/-2.57E-05 QCI203694012 LCS Lead-210 0.00953 Uncertainty QC1203694009 MB Lead-210 Uncertainty QCI203694011 410794002 MS Lead-210 0.0355 0.00128 Uncertainty +/-2.57E-05 Notes: u Counting Uncertainty is calculated at the 68% confidence level (!-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product +/-8.19E-07 0.0145 +/-0.00017 0.0013 +/-2.36E-05 0.0109 +/-0.000157 -7.02E-06 +/-1.30E-05 0.0428 +/-0.000647 uCi/kg uCi/kg 1.5 uCi/kg uCi/kg uCi/kg A B BD c D F H K L M M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Matrix Related Failure N/A RPD or %Recovery limits do not apply. Nl See case narrative ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Q One or more quality control criteria have not been met. Refer to the applicable narrative orDER. REC% Ran e Anlst Page 2 of Date Time 103 (75%-125%) KSDI 12/15/16 13:4• (0%-20%) KSD1 12/28/16 09:1• 115 (75%-125%) 12/28/16 07:2· 12/28/16 09: I 117 (75%-125%) 12/28/16 07:2· GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407-(843) 556-8171 -www.gel.com QC Summary Workorder: 410794 Page 3 of NOM Sample ual .~---=----~~----=--R:.=..P:::.D:...:o/c:.=o _ _:,RE=cC::::_0.:..,:Vo:.___.;:.:R:=ac:.n:~e Anlst Date Time Parmname R u UI UJ UL X y 1\ h Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded N/A indicates that spike recovery limit do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. "The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) i evaluated against the acceptance criteria when the sample i greater than five times (5X) the contract required detection limit (RL). ln cases where either the sample or duplicate value is less than 5X the RL a control limit of+/-the RL is used to evaluate rhe DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDILT results, the values listed are the mea ured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. ATTACHMENTG STACK SAMPLE LABORATORY RESULTS , J j J Prepared for: Energy Fuels Resources 642SSHwy91 Blanding, Utah 84511 Date of Report: December 1, 2016 TIDRD QUARTER RADIONUCLIDE EMISSIONS TEST CONDUCTED AT ENERGY FUELS RESOURCES SOUTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE GRIZZLY BAGHOUSE BLANDING, UTAH August 22-24, 2016 By: TETCO 391 East 620 South American Fork, UT 84003 Phone (801) 492-9106 Fax (801) 492-9107 fax ] CERTIFICATION OF REPORT INTEGRITY Technical Emissions Testing Company (TETCO) certifies that this report represents the truth as well as can be derived by the methods employed. Every effort was made to obtain accurate and representative data and to comply with procedures set forth in the Federal Register. 1 /1! ~ Mike McNamara A4A 11 ~--~ Reviewer: I vv~ v v ~------~----------------- Date: ___ \_"2_-_1_--_2_{)_1_b ____ _ Dean Kitchen Reviewer: ~~ --------~,~~~~~------- Date: ____ I"-""A_---';:~-("--'~--- ii ., TABLE OF CONTENTS PAGE Introduction Test Purpose ......................................................................................................................... ! Test Location and Type of Process ...................................................................................... ! Test Dates ............................................................................................. " ................................ 1 Pollutants Tested and Methods Applied .............................................................................. 1 Test Participants ................................................................................................................... 2 Deviations from EPA Methods ............................................................................................ 2 Quality Assurance ................................................................................................................ 2 Summary of Results Emission Results .................................................................................................................. 3 Process Data ......................................................................................................................... 3 Description of Collected Samples ........................................................................................ 3 Discussion of Errors or Irregularities ................................................................................... 3 Percent Isokinetic Sampling ................................................................................................ 4 Source Operation Process Control Devices Operation ..................................................................................... 5 Process Representativeness .................................................................................................. 5 Sampling and Analysis Procedures Sampling Port Location ....................................................................................................... 6 Sampling Point Location ...................................................................................................... 6 Sampling Train Description ................................................................................................. 7 Sampling and Analytical Procedures ................................................................................... 7 Quality Assurance ................................................................................................................ 7 Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence iii LIST OF TABLES PAGE Table I Measured Radionuclide Emissions ..................................................................................... .3 II Percent Isokinetic Saiilpling ................................................................................................ 4 III Saiilpling Point Location ...................................................................................................... 6 IV Complete Results, South Yell ow Cake Scrubber .............................................. Appendix A V Complete Results, Yellow Cake Dryer Baghouse ............................................. Appendix A VI Complete Results, Grizzly Baghouse ................................................ Appendix A LIST OF FIGURES Figure 1 Facility Schematic Representation South Yell ow Cake Scrubber ..................... Appendix D 2 Facility Schematic Representation Yellow Cake Dryer Baghouse .................... Appendix D 3 Facility Schematic Representation Grizzly Baghouse ... ...... .. . . . . . .. .. . ...... Appendix D 4 Schematic of Method 5/114 Sampling Train ..................................................... Appendix E ] iv J ] INTRODUCTION Test Purpose This test project was conducted to determine the total radionuclide emissions from the South Yellow Cake Scrubber, the Yellow Cake Dryer Baghouse and the Grizzly Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dscf). Test Location and Type of Process Energy Fuels Resources is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Yellow Cake Dryer Baghouse. The packaging enclosure also discharges into the Yellow Cake Dryer Baghouse. The South Yellow Cake (SYC) dryer was the only operating dryer at the time of the test. The North Yellow Cake dryer is currently not operational. The Grizzly Baghouse serves as the main dust control device for the raw ore unloading and conveying to the processing building. Stack schematics are shown as Figures 1 - 3 in Appendix D. Test Dates The first test run on the SYC Scrubber was completed August 23, 2016 and the second run on August 24,2016. One run was completed on the Yellow Cake Dryer Baghouse August 22,2016 One run was completed on the Grizzly Baghouse August 23 2016. Pollutants Tested and Methods Applied The tests were a determination ofradionuclide emissions in accordance with EPA Method 5/114. Test run filters and front wash residues were sent to Test America located in Richland, Washington for radionuclide analysis. Test Participants Test Facility Division of Waste Management and Radiation Control TETCO Deviations from EPA Methods None. Quality Assurance Logan Shumway Phil Goble Mike McNamara Kawai McNamara Ryan Johnson Doug Olsen Jeff Graton Testing procedures and sample recovery techniques were according to those outlined in the Federal Register and the Quality Assurance Handbook for Air Pollution Measurement Systems. 2 SUMMARY OF RESULTS Emission Results Table I presents the findings of the test in Curies per dry standard cubic foot. Tables IV, V and VI in Appendix A have more detailed information. Table I. Measured Radionuclide Emissions South Yellow Cake Yellow Cake Baghouse Grizzly Baghouse Run# Scrubber Test run 1 on the Yellow Cake Dryer Baghouse was completed with 6 barrels being filled. Process Data The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow and pressure drop readings (LU>) were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings ( 6P) were recorded and are found on the test run sheets. Tons per hour of material and belt speed for the Grizzly Baghouse are found in Appendix D. Production data was retained by Energy Fuels Resources. Description of Collected Samples The test filters for the South Yell ow Cake Scrubber were heavily covered with a white colored particulate. The front washes were cloudy in appearance. The test filters for the Yellow Cake Dryer Baghouse showed no visible particulate matter. The front wash was clear in appearance. The test filters for the Grizzly Baghouse showed no visible particulate matter. The front washes was clear in appearance. Discussion of Errors or Irregularities None 3 J Percent Isokinetic Sampling Each test run was isokinetic within the ±10% of 100% criterion specified in the Federal Register. Isokinetic values for each test run are presented in Table II. Run# South Yell ow Cake Yellow Cake Baghouse Grizzly Baghouse Scrubber 1 98 98 98 2 101 4 ] SOURCE OPERATION Process Control Devices Operation All process control devices were operated normally. Recorded scrubber water flow, pressure, and baghouse 6P readings were recorded and are found on the test run sheets or in Appendix D. Process Representativeness The facility was operated normally. Production data was retained by Energy Fuels Resources. 5 J ' .. . •! ' ' . ' J SAMPLING AND ANALYSIS PROCEDURES Sampling Port Location The inside diameter of the South Yellow Cake Scrubber stack is 12.75 inches. The two, four-inch diameter sample port are located 28.24 diameters (30 feet) downstream from the last disturbance and 6.59 diameters (7 feet) upstream from the next disturbance. Figure 1 in Appendix Dis a schematic of the stack. The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch diameter sample ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 2 in Appendix D. The inside diameter of the Grizzly Baghouse stack is 18.75 There are two, three-inch diameter sample ports located 2.56 diameters (48 inches) downstream from the last disturbance and 1.31 diameters (24.5inches) upstream from the last disturbance. The sample port locations are depicted in Figure 3 in Appendix D. Sampling Point Location Table III shows the distance of each sampling point from the inside wall according to EPA Method 1. Each point was marked and identified with a wrapping of glass tape and numbered . These points were determined by measuring the distance from the inside wall. Sample Point 1 2 3 4 5 6 7 8 9 10 11 12 SYC Scrubber 0.85 3.19 9.56 11.90 Point Location ,.co ... ~ .... ,. .. (Inches) from Inside Wall 6 Yell ow Cake B 0.70 2.34 4.74 11.26 13.66 15.30 0.50 1.26 2.21 3.32 4.69 6.68 12.08 14.06 15.43 16.54 17.48 18.25 Sampling Train Description To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-5/114 were followed. All sampling trains were made of inert materials, (Teflon, stainless steel, and glass) to prevent interference of the sampled gas and particulate. The stack analyzers used to conduct Methods 1- 5/114 were constructed to meet the specifications outlined in the CFR. The temperature sensors were K-type thermocouples. Heater, vacuum, and pitot line connections were designed to be interchangeable with all units used by the tester. A 316 stainless steel probe liner was used for the tests. Figure 4 in Appendix E is a sketch of the Methods 5/114 sampling train. Sample boxes were prepared for testing by following the prescribed procedures outlined in Methods 5/114. Sampling and Analytical Procedures All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 5/114. Quality Assurance All equipment setup, sampling procedures, sample recovery, and equipment calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbook for Air Pollution Measurement Systems. 7 l l i '' J ... ] , ] ] j APPENDICES A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence 8 ] ] 1 J ] 1 I J APPENDIX A Table IV Complete Results, South Yellow Cake Scrubber Table V Complete Results, Yell ow Cake Dryer Baghouse Table VI Complete Results, Grizzly Baghouse Nomenclature Sample Equations A TABLE IV COMPLETE RESULTS ENERGY FUELS CORPORATION, BLANDING. UTAH .. , SOUTH YELLOWCAKE SCRUBBER Symbol DescriEtion Dimensions Run#l Run#2 Date 8/23/2016 8/24\16 ., Filter# 6707 6709 Begin Time Test Began 8:18 11:48 End Time Test Ended 16:27 19:50 Pbm Meter Barometric Pressure ln. Hg. Abs 24.50 "24.55 AH Orifice Pressure Drop ln.H10 1.053 0.948 y Meter Calibmtion Y Factor dimensionless 0.995 0.995 Vm Volume Gas Sampled-Meter Conditions cf 326.878 318.359 Tm Avg Meter Tempemture "F 82.2 81.3 --JAP Sq Root Velocity Head Root ln. H20 0.3625 0.3459 Wt,_c Weight Water Collected Grams 160.3 164.3 Tt Duration of Test Minutes 480 480 cp Pitot Tube Coefficient Dimensionless 0.84 0.84 Dn Nozzle Diameter Inches 0.3130 0.3130 C02 Volume% Carbon DioK.ide Percent 2.40 3.00 02 Volume% O><ygen Percent 16.40 15.60 N2&CO Volume% Nitrogen and Cllfbon Manmade Percent 81.:20 81.40 Vmstd Volume Gas Sampled (Standard) dscf :260.171 254.248 Vw Volume Water Vapor scf 7.558 7.747 Bw, (measured) Fraction H20 in Stack Gas (Measured) Fraction 0.028 0.030 Bw, (saruraJed) Fraction H10 in Stack Gas (Saturated) Fraction 0.098 0.107 Bw, Fraction H20 in Stack Gas * Fraction 0.028 0.030 xd Fraction of Dry Gas Fraction 0.972 0.970 Md Molecular Wt. Dry Gas lbllbmol 29.04 29.10 M. Molecular Wt. Stack Gas lbllbmol 28.73 28.78 %1 Percent lsokinetic Percent 97.8 100.6 AVG T, Avg Stack Temperature "F 107.2 110.3 108.8 A. Stack Cross Sectional Area Sq. Ft. 0.887 0.887 Pa Stack Static Pressure ln.Hp -0.075 -0.075 PbP Sample Port Barometric Pressure ln. Hg Abs 24.43 24.48 P. Stack Pressure ln. Hg Abs 24.424 24.474 Q, Stack Gas Volumetric Flow Rate (Std) dsclin 9.20E+02 8.74E+02 8.97E+02 Oa Stack Gas VolUlnclric Flow Rate (Actual) cl\n L25E+03 l.l9E+03 1.22E+03 v. Velocity of Stack Gas fpm 1.40E+03 1.34E+03 1.37E+03 Curies Radionuclides per sample pCi 2221.5 4036.4 Crad Concentration of Radionuclides pCildsef 8.539 15.876 l2.207 ERrad Emission Rate ofRadionuclides pCilhr 4 .712E+05 8.328E+05 6.520E+05 * If the measured moisture content is greater than the saturated moisture level (supersaturated), the saturated moisture value will be used in all calculations ( 40 CFR 60, Method 4, Section 12.1. 7). TABLE V COMPLETE RESULTS, PM ENERGY FUELS CORPORATION, BLANDING, UTAH YELLOW CAKE DRYER BAGHOUSE Symbol DescriEtion Dimensions Run #1 Date Date 8/22/2016 J Filter# 6704 Begin Time Test Began 13:33 End Time Test Ended 15:35 Pbm Meter Barometric Pressure ln. Hg. Abs 24.50 ~H Orifice Pressure Drop Jn.H10 1.578 y Meter Calibration Y Factor dimensionless 1.004 Vm Volume Gas Sampled-Meter Conditions cf 94.829 Tm Avg Meter Temperature "F 78.3 ...j~p Sq Root Velocity Head Root ln. H20 0.6673 Wt,.c Weight Water Collected Grams 25.0 Tt Duration of Test Minutes 120 cp Pilot Tube Coefficient Dimensionless 0.84 Dn Nozzle Diameter Inches 0.2505 C02 Volume% Carbon Dioxide Percent 0.00 02 Volume % O~ygen Percent 20.90 N 2 &CO Volume% Nitrogen and Carbon Monoxide Percent 79.10 Vmstd Volume Gas Sampled (Standard) dscf 76.832 Vw Volume Water Vapor scf 1.179 Bw. Fraction H10 in Stack Gas Fraction 0.015 xd Fraction of Dry Gas Fraction 0.985 Md Molecular Wt. Dry Gas Jbllbmol 28.84 Ms Molecular Wt. Stack Gas lbllbmol 28.67 %1 Percent lsokinetic Percent 97.5 T, Av~: Stack Temperature OF 116.9 A, Stack Cross Sectional Area Sq. Ft. 1.396 Pa Stack Static Pressure ln.H10 -0.49 PbP Sample Port Barometric Pressure ln. Hg. Abs 24.43 P, Stack Pressure ln. Hg. Abs 24.394 Q. Stack Gas Volumetric Flow Rate (Std) dscfin 2.68E+03 Qa Stack Gas Volumetric Flow Rate (Actual) cfin 3.65E+03 v. Velocity of Stack Gas fpm 2.61E+03 Curies Radionuclides per sample pCi 8805.8 Crad Concentration of Radionuclides pCildscf 114.6112 ERrad Emission Rate of Radionuclides pCilhr l.842E+07 '•I TABLE VI COMPLETE RESULTS, PM ENERGY FUELS CORPORATION GRIZZLY BAG HOUSE S~mbol DescriEtion Dimensions Run #I Date Date 8/23/2016 Filter# 6706 Begin Time Test Began 8:46 End Time Test Ended 16:51 Pbm Meter Barometric Pressure ln. Hg. Abs 24.50 6H Orifice Presst.ae Drop ln. H20 1.624 y Meter Calibration Y Factor dimensionless 1.004 Vm Volume Gas Sampled-Meter Conditions cf 384.450 Tm Avg Meter Temperature "F 83.9 ...f6P Sq Root Velocity Head Root ln. H20 0.4179 Wfwc Weight Water Collected Grams 86.2 T, Duration of Test Minutes 480 cp Pilot Tube Coefficient Dimensionless 0.84 Dn Nozzle Diameter Inches 0.3100 C02 Volume %Carbon Dioxide Percent 0.00 02 Volume% Oxygen Percent 20.90 N 2 &CO Volume% Nitrogen and Carbon Monoxide Percent 79.10 Vmstd Volume Gas Sampled (Standard) dscf 308.323 Vw Volume Water Vapor scf 4.064 Bw5 Fraction H20 in Stack Gas Fraclion 0.013 xd Fraction of Dry Gas Fraction 0.987 Md Molecular Wt. Dry Gas lbllbmol 28.84 • J i'' Ms Molecular Wt. Stack Gas Jbllbmol 28.70 ·~'~ %1 Percent Jsokinetic Percent 98.1 T, Avg Stack Temperature "F 77.0 A, Stack Cross Sectional Area Sq. Ft. 1.917 Po Stack Static Pressure ln. H20 -.15 Pbp Sample Port Barometric Pressure ln. Hg. Abs 24.47 Ps Stack Pressure ln. Hg. Abs 24.459 Q. Stack Gas Volumetric Flow Rate {Std) dscfm 2.40E+03 I Oa Stack Gas Volumetric Flow Rate (Ac(Ua() cfin 3 .02E+03 I ... , v. Velocity of Stack Gas fpm 1.58E+03 -~ ,, Curies Radionuc\ides per sample 2.0 l pCi Crad Concentration of Radionuclides pCildscf 0.0066 ERrad Emission Rate of Radionuclides pCi/hr 9.509E+02 ~ .,, I II j J Method 5 Nomenclature %1 = percent isokinetic as a percent As = stack cross-sectional area (ft3) ASdP =seem Btu = unit heat value (British thermal unit) Bws = fraction of water in stack gas Cf = concentration of front half particulate matter (gr/dscf, lb/dscf, etc.) CmeLal = concentration of metals (ppm, p,g/ft3, etc.). Atomic symbol replaces "metal" C02 = percent carbon dioxide in the stack gas Cp = Pitot tube coefficient Cx (avg) = average concentration of x Cx (corr) = concentration of x corrected to the required percent 02 Deq = equivalent diameter for rectangular stack Mf = orifice pressure drop (inches H20) Mi® = orifice pressure (inches H20) Dn = nozzle diameter (inches) Dn des = calculated desired nozzle size (inches) dP = stack flow pressure differential (inches H20) Ds = diameter of the stack (feet) EA = percent excess air ERf = emission rate of front half particulate (lblhr) ERmrnBtu = emission rate per mmBtu or ton of fuel etc. ERx = emission rate of compound. Specific compound replaces x K-fact = multiplier of test point dP to determine test point Mf L = length of rectangular stack (inches) mBtu = thousand Btu Md = molecular weight of stack gas, dry basis (lbllb-mol) Mf = mass of particulate on filter (mg) Mfp = mass of particulate matter on filter and probe (mg) rnrnBtu = million Btu Mp = mass of particulate matter in probe (mg) Ms = molecular weight of stack gas, wet basis (g/gmol) N2 = percent nitrogen in the stack gas 02 = percent oxygen in the stack gas .JMi = average of the square roots of dP (may also be referred to as ASdP) Pbm = absolute barometric pressure at the dry gas meter (inches Hg) Pbp = absolute barometric pressure at the sample location (inches Hg) Pa = stack static pressure (inches H20) P5 = absolute stack pressure (inches Hg) Pstd = absolute pressure at standard conditions (29.92 inches Hg.) (J = time length of test (minutes) Qa = stack gas volumetric flow rate (acfm) Q5 = stack gas volumetric flow rate (dscfm) Qw = wet stack gas std. volumetric flow (ft3/min, wscfm) T m = meter temperature (°F) T5 = stack temperature (°F) Tstd = absolute temperature at standard conditions (528°R) Tt =see (J Vm = sample volume (ft3) at meter conditions I J ., J ] Method 5 Nomenclature Vmstd = volume standard (dscf), sample volume adjusted to 68°F and 29.92 inches Hg. V 5 = velocity of stack gas (fpm) Vw = volume water vapor (scf) at 68°F and 29.92 inches Hg. W = width of rectangular stack (inches) Wtwc = weight of the condensed water collected (grams) ~ = fraction of dry gas Y = meter calibration Y-factor (dimensionless) ..., > ' ..J l j "\ J 1 J Method 5 Sample Equations Vmstd · (Ts +460) · 1039 %1 = 2 8·Vs·Ps·~·Dn D2n As= -5 -4 Yw Bws = ----Vmscd+Vw Mfp · 0.01543 Cr = ---''----Vmstd 20.9 -desired %02 Cx (corr) = Cx (avg). 20.9-actual %02 2·L·W Deq = L W ~~--------~===== 0.0269 · (Pbm +0.0735) (Ts +460) · Ms Dndes = (Tm +460) ·Cp ·Xi Ps ·&> %02 -0.5 ·%CO EA= -------~----------~ 0.264 · %N2-(%02-0.5 ·%CO) ERr = Cf · Os · 0.00857 ERx ERmmBiu = rnmBtu/hr 846.72 · Dn4 · Llli@ · C2 ·X~· Md · Ps · (Tm +460) K-fact = P AH Ms · (Ts +460) · (Pbm + m) Md = C02 · 0.44 + 02 · 0.32 + N2 · 0.28 Ms = Md · ~ + 18 · Bws Po Ps = Pbp+--13.6 Qa = Vs ·As On · ~ · Ps · Tstd Os= ------(Ts +460) · Ps1d Os Qw= ~ Vw = Wtwc·0.04715 ~ = 1-Bws .. 1 J ] APPENDIXB South Yellow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data Yellow Cake Dryer Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data Grizzly Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data B Prelim 6 pts blank Facility Energy Fuels Stack Identification Yellow Cake Dryer Baghouse Date , l Barometric Pressure B Pbm in Hg PbP in Hg N Static Pressure (Pa) inH10 A Estimated Moisture (Bw5) I % Sample Height from Ground feet 1 Comments: Stack Dia. 16 Reference: 0 Ports are 57" Upstream !Tom next disturbance Ports are 468" Downstream !Tom last disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B c D E F I 4.4 0.70 0.70 2 14.6 2.34 2.34 3 29.6 4.74 4.74 4 70.4 11.26 11.26 5 85.4 13.66 13.66 6 95.6 15.30 15.30 Averages: Ts LFlow -------- ~P ___ _ "1/~p ---- KEY=> B ~ z:aoA 2~0 ~-·~-~i:::.t: ~-Pield Data Sheet Plant Ener~uels Date: 'd/2 1\ b • TriYeBe Time 1 1 1 2 2 2 3 3 3 4 4 4 1 1 1 2 2 2 3 3 3 4 4 4 "'----' :;. ~-_l :.:.._ •• -J • ·~ ..... --~~··~ .-.;..;.:;~T· ~- TETCO Filtc:r fo1 6'1 Sample Box._ku....._ C,10~ Location: South Yellow Cake Dryer Scrubber Operator: j\rE ui,P.J'6N DGM t.P t.H I"'Ho0l Vacuum DGMTempfT,.) !ft'J Total :.'2.1.'\~~ ~ ..J &.iq~S...I' 2S.~../ 2Si'3 ./ 3"\Yi ../ ~2..2. ~),(,. ?:> 7t> ·o/ Average ..Jo.~2.!; \.053 \01 .2.. -------------- DGM before leak Check Rate (ft3/mln) DGM After Leak Check '\1~.~~!; f"'.OO& q,~ .~\'E> -~·~:~~~: Page _j_or---1.-Run 11j_ .() i N Stack Diameter 12.75" Port Reference _,0'--"--- Ports are 7' Upstream from next disturbance Ports are 30' Downstream from last disturbance Assumed Moisture Probe ~ Nozzle Calibnltion 4-6% Cp 0.84 ~ ~ .::m_ :illL AvgD.~ inches Gas Bag E. •() S Console~ Y-Factor 0. ~«} S L\HCD I, S•n in HzO Barometric Pressures Pb.,LL.f, SO in Hg Pb,. "l.'f. "'~ in Hg P0 -.OJS. inH20 LeaJc Check: Pre Post ft'hnin o.ooa vacinHg~ Pilol Rate ....o.:.Q lnH,O ~ Water Collected 0.002.. ~ ~ ~ ~ _...........i,__& Time Sampled '4 2.0 min Review _..,:J~Gz~---- K= @T,. K= @T,. J<:, \'l:'-1""' '\,~ .b\0 l, aSS _:::_ . ,..._ -' -.. ~ .. ttr"-~; I;-:1:.». -; M.S. Field Data Shert . Plant: Energy Fuels Date: B/2.-i/Lio T111>ene II Time --r-DGM .6P "":'-1 --- TETCO Filter fo, tl ~ Sample Box._H'-'--- Locution: South Yellow Cake Dryer Scrubber Operator: jf.f~ ~~h'ToN II .6H ':" H,OJ II Vocuum II 1 Ten:peratures ~~ 1 II DGM T~ (T,.) ~ ;. ~-:::~~li~t· Page_l_or_\_ Run#_k_ r 8 6 N Stack Diameter I 2. 75" Port Reference _,0'-"--- Ports are 7' Upstream from next disturbance Ports are 30' Downstream from last disturbance Assumed Moisture 4-6 % Probe \~I;, Cp 0.84 Nozzle Calibration .'"!:t\3 .~\'~ 11,\"!, ~ Avg D •• :,\'\0 inches Gas Bag t..:..oJ. Console~ Y-Factor 0 I 9q S .6He~ ~ in H20 Barometric Pressures Pbm2~.55 inHg Pb0 "2. It • ~~ in Hg PG -• 0 '"\ 5 in H20 Leak Check: Pre Post n'tminO.oot'\ o.~l VIC in Hg '2.o 1 0 ~0 Pilot !Ute O 1 Q ..Q& lnH10 ~.o qlf) Water Collected I(,~' 3 g ~ Time Sampled 4<rs D min '?l~oo Review ....i( ... 3\~ .~s~ ..t; ~.3o, l ../ 2'2;-a\o ./ 2.fo1f 7 / Total Average -Jo:!>'-1 S, O,C\'fS ilo.~ Sl. 3 DGM before Leak Check Vac ("Hg) Rate (ft3/mln) DGM After Leak Check ---------·---··-- Rate (ft3/min) K= K= @Tm @Tm Prelim 6 pts blank Facility Energy Fuels Stack Identification Yellow Cake Dryer Baghouse Date r Barometric Pressure B Pbm in Hg PbP in Hg N Static Pressure (P0) in H20 A Estimated Moisture (8w5) I % Sample Height from Ground feet Comments: Stack Dia. 16 Reterence: 0 Ports are 57" Upstream from next disturbance Ports are 468" Downstream from last disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B c D E F I 4.4 0.70 0.70 2 14.6 2.34 2.34 3 29.6 4.74 4.74 4 70.4 11.26 11.26 5 85.4 13.66 13.66 6 95.6 15.30 15.30 Averages: Ts LFiow --------L\P ___ _ ..JL\P ---- KEY=> L\P L Flowl ~ Field Datu Sheet Plant: Energy Fuels Resources, lllnnding, UT Date: e ( 2:Z ( z 0 I \, TETCO Filter f.. 70<-( Sample Box~ Locution: North Yellowcake Dryer Baghouse Operator: M. ,s.H,.J.d,!Mcr.lb- TIIY<Be Time DGM 6P 6H (IIH,O) Vacuum Temperatures m """" Clock Min (6} (A'• (in liP, Desired Actual , .. ,~,. Stack (T,) Probe Probe Oul Filter Effillellt ~ 1 ,, !3.J 0 ~5 .S'i1 .3~ I .1.'{ \. 'l 'i 3 II'S' 2t,o 1, !:J. t{i--L~ 2 IQ "lz. et.r .)"j 1·~1 ··~"1 3 ~~~ "Z.G.O ZC!!l' -zc..{ 56 3 1,.0 5e ,I(,(' • '10 I· "tl l. '<I 3 11 ... lwl' 'l. ~ l 'Z. ~ ( Sa. 4 10 . S1·1t.O 'c.{ 0 \• "<I l· '4( ..3 Ill. • 2.11!0 2 ,.,-1 z .. -:r {~ 5 lot() I..S·'L31 •:) (., l· ~'1 \·11 3 •If 2. '{o -z.,r? Z,fl) .5.) 6 Stl "Jl.. ~ l<" • '3"( t.-z.o lotO 3 tlf '"{ J,{Y Z-£f St. e 1 '"': 3.5 t.o 19 .l.).J. •S'S' 1.93 1·93 'i 111-Zt.{ 'Z,~(, Z'{). 5.5 2 "1'<> g't.'\<tJt) .ft.-l· 8~ '· tl3 ~ lit Z7o "'2-::Y:., Z:lCf 54 3 eo 'fl...~ lfo '52.. l·h ,, ~:) ~ lit 2.taf' Z.3~ ~")+-6~ 4 ~Q LoS·I{O · Sl l.,, t.?"t ~ liS 1.10 Z"40 Z..C-iO 5+- 5 \oo (1~.5~{ •ll ,,,, t•""R '{ II" z{f' Z'is' 7-'ii sa 6 uo (1.1,.cS'S' .so l·1 <. (·1~ "' \"1.0 !{t,o l'ir. '-If \a C,Q ls:s( I 'tO 13 0 .)'7{, --- Total "'{ • '8 L 't -1 <6 -coS .I ,~.'{~1)/ \ j OJ/ ~ .J 0.1.<11~ \. ~1 ~ \l \t' ~ AvcBge ClllllmCIIIs: Time BaghouseAP Time BaghouseAP \\ ~\{~ 1~'.31{ L.'f i'f ;\ 1·11- ,~:~ l·b1 '~ ·.sq 1.1\ 1'1'·~ L_ 1 · lp \ I S'.l) 1..1v. - DGM Temp(T..) Out In (,Cf '~ ll l..!f 7T c., 8.3 lO it, "71 8":l. ""JZ.., 111" '7..3 cas ,..., 8<y I I.( '\O -,:r (it l !f' <fL. 7(, -- 167'!./ ~~-3 \ I Page_ -of --Run"-~-- B i t Ao N Stack Diameter 16" __ Port Reference _0.0"_ Ports are Pons an: ~Upstream fmm next disturbance 468" Downstream from lost tlisturbtlnce Assumed Moisture ---'--% Probe ~ CJl~ No7.7.lc Calihrotiun .-zfc .z.n .z.ro .z.to Avco •• ~ror-i~ Gas Bag Ambient Air Console_,_,__ __ Y-Faclor~ hHa ~ inH20 Ournmetric l'~ures Pb,. 1. t{. V Pb. Z"i·'l~ Pu -• ~1 Leak Check: Pre inHg in Hg inHp ~ ft'lmm l). oas VKiniiG lf. 0 6>. oo'l.. 10·0 Pi101R.,o 0·0 o.O )nii,O 7•0 ~ Water Collected ZC. 0 _ __;::.._ _____ & Time Somrlcd 11.o min Review NJJ}JA. K= K: @Tm @T. .. Prelim 12 pts blank Facility Denison Mines Stack Identification Grizzli: Baghouse Date Bjz3 r Barometric Pressure Pbm l.LI,)O in Hg PbP 2.. '-4 I 4 ':l. in Hg N AOB Static Pressure (P0 ) -,f) in H20 Estimated Moisture (Bw,) I '70 Sample Height from Ground 3'0 feet Comments: Stack Dia 18.75 Reference: 3.0 Must use 36" probe or lon~er to keee box outside handrail Ports are 24.5" Upstreum from next disturbance Ports are 48" Downstream from last disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B c D E F I 2.1 0.50 3.50 2 6.7 1.26 4.26 'TO .l"l 3 11.8 2.21 5.21 4 17.7 3.32 6.32 70 ·11 5 25.0 4.69 7.69 6 35.6 6.68 9.68 .,l ·~~ 7 64.4 12.08 15.08 8 75.0 14.06 17.06 "'1/ L L"O 9 8?.3 15.43 18.43 10 88.2 16.54 19.54 'II I 1-=j- II 93.2 17.48 20:48 12 97.9 18.25 21.25 Averages: Ts L. Flow ---- LlP --../t,p -------- KEY=> ~~T_s ____ ~6~P--L. __ F_Io_w~~ &' · '~,~ 0aiD she.:t Pion!. ..QerrisOH IPIIn'Cs £'~ ~l) Dale: e{~}(tol~ Tr:~w:nc. T1me DGM l>.P Porn I Clock Min(B} (li'J , .. u.o• " ~ 1 e·.'js 0 't31.1~fl ·I If 2 to 9~1D·~O .J'l 3 ~0 f>(o 1.. 9oS ,2.0 l,lo.( 4 (.o 8eo 'L "TO .1._t 5 So !> '" . 'i oo ''L '-1 6 loO -~' 5 . 5_(,() • 'to~ (1,( 7 110 C{~'). ~of • JCl 8 )'(O qs~ .-s"o ·I_£_ 9 '"0 Gi'-+ .tto •18 ') "' 10 18o C\8~. C.~{ ·I"~ 11 Zoo «'il:f 'l s Z{ • I C, 12 2'20 0 f5.DCJ0 .J <. Ott ,( 1 n:.ft zqo O~O.'f~ ·l\ 2 Z(.,O o'\ ~. ~~t • Jl 3 Z.~D o5t'te-.36( ·I~ ~ ,( 4 3oo 010 ..... t< ·I~ 5 3to g 8'\.11.0 . '"' 6 .J~o o~'\.'\tto • ((c. '-V7 ~C..o 115. "t1(' r1..\ 8 380 ·~ l .'151S .. ~o 9 'ioO t "l ct. t:t 'W -18 "\ V10 4fW 't. (p_t5S .,, 11 '1<40 18 2..~o0 . ,, 12 .. ,0 l't~30 ,(j_ \~'.(l Lf~O 1.1!,q. • 21B / ~Hl .. K..OJ Desrred Actual l.~~ I.-e~ 1.?-'1 1 ... ~., '·~~ I. '03 '· 1"'-(.CfL_ 1..(' 1.. I c, 'Z.·II '~-· Jt 1.1'( l·1'{ l. t. 'l-l·~l- L· <.l-l· ~ ';J. H'f> 1,18 \.1~ [.'1, '. 4(9 ,, .. , f. o1-l·o'l.. t.o2. ,,.,'Z. 1-l't l-li 1·1~ l·l9 1·'(1-l·.q '·1'1-'·~'"f' t .,.r J. ttf 1·85 I·Y,( ,.~(, H.(, L.1{ t.1i 1-1-r t··H~ 1·"1{ t.({ '"-~-__ 1 ~~ filler ~ 1 ,;t; LoC<~uon: Grizzly Baehous~ Operator: tv\. M.~\l~""-lo- Voc:uum Tempcca!Ures rr1 (•llt=J Slack (T,i Probe ProbcOOI Filter 3 11 Z'{) Zro Zlo 3 ,, 1.~1 Z<..t 41 3 ,I l. 'to Z1l 15\ 3 ~2. t 'too l-<L 2.{L ~ ,3 ZC.( 2.){., -z:s~ "' ,"{ tq"' zc~ tf~ "' 1"\ '1. '3o "l.Coi~ 2.tf;. 3 1i !"{+ Z!1· t-f~ 3 "7~ Z'-o Z(,C( 'Z.. f.,C( 3 go ~n. 'l. !'0 z.ta j 8( 24[~ 'l.'(O z s'(.. .) 8( 2~l 'l.{''{ ti'\{ 3 9t z.q"' Z.f'i Z.{'{ 3 83 2 ~'1 '2.-$" l. 2.)1... _"3 et.t 'Z"i1-·'l.{L! z{L( 3 ?,( 2.30 zze 'Z.Z. ~ 3 15 l.t.'{ Z.'?c 21o ~ 11 1."70 zi4 2{'f ~ 1~ 'l.-70 Z.b'f U"t 3 _80 l {_~ 1.,G,(o 1-'--~ '-{ %0 1.10 '2..~"1 Z.l.f';f .3 15 1.'i1 2.(0 Z{(j 3 11 z.'ie Z.{l ?.{{ _3 ,'i !.i, l.i'1 Z1( , Emuent _5_1- 5-z.. 5Z- 55 5":J.. 5"+ se qq S_l 51- 5.3 S"( '-o Si{ 5'1_ 5z. 52. ii'Z. 54 5C. 5'Z- S'-1 5Y 5'1 Tolal jSY. L\50~ \0·61.. '\'tv" ~8-~l'D ~'{CII,. ll.o Average .J o-"\\1, l-.1,. 1.'-\ COfi\IMniS." -j .J !' DGM Temp (T .) Out In C-Cf (.~ ,~ (.,, B~ ,1- 8't' 1-f" Cfv '1-r ,t. So *f~ Bt ~, 8(,. 'i_i_ __S:o_ Cf' gq -=fl.( Bey i3 ~, 8~ g':J. cro S(g ,3 81- 8'( 8{. g5_ ~2. s~ 8o ~-3 IR 13) 1/lJ 83 1e FH 1( ~0 T1 BD .,.., 4~1.'0/ '6). ~ Rlllll: \ i AOB N Slack Dtameler 18. 75" Pan Reference ___lj!:_ Pons are 24.5" Upstream from ne~t disturbance Pons arc 46" Down~trcam from last dosturbancc Assumed MuisiUrc 1 % Probe Je(,-1.. Cp~ Nozzle Calibration ~ IJIO _•_3_10 __ •_3_10_ A~g D. • 310 tnches Gas Bag Ambient Air Console.......:Cf~-- y -Factor I· OO't 6H111 ~ mH10 Barometric Pressu= Pbm l({. {O Pbr Z I.{, I.(~ - tn Hg inHg Po -•I 2 m H10 Lo>kChcok: Pre n'/n•n 0 -803 vxinHg z:z.., PotOI Rote () · '\) 1n H,o {j,·() Waler Collected Tim.: Sampled Review Post l) ·c:l~l{ ...11& o-O ~ i(.b.l_ ___j!O ~ K= K= @Tm @Tm g mm l J South Yellow Cake Scrubber Sample Recovery Gas Analysis Data (ORSAT) Yellow Cake Dryer Baghouse Sample Recovery Gas Analysis Data (Ambient) Grizzly Baghouse Sample Recovery Gas Analysis Data (Ambient) Lab Analysis Chain of Custody APPENDIXC c I • Facility: ~lre'S' C"li~y J Stack Identification: SYC Scrubber ~~~~~------------------------- IMPINGERS Filter Number: C&,7o"-t fo1o ~ IMPINGERS Filter Number: bloC\ IMPINGERS Filter Number: ·------·· ---·-·--· Run: [ Sample Box: k1 lmpinger Number 1 SG \ loO. '?:> v-Q /7 rl I -, I ; . IIi. A-u -.., Z.v , Y; ~-::.-----•• w--·-•-•~ ------ Run: 2. Sample Box: H 1 2 lmpinger Number I 3 I 4 I s 6 Initial Volume of liquid (H20) in impingcrs, (ml) so Final (g) --l;oj~....__-+~!.....=._--4-o<l...:....::_~l-=....::::j~-I-~.....J,...:.~4-J--1....~--'l. Initial (g) --"'~~,-+.3oLL..LJt.....L-4-:..:..;;;....,!~~=~-+::..=;,;;:..:..._.!-~~:,....-=­ Net (g) ====~======~~~~6=====~~===6~~~ Run: Sample Box: 1 2 lmpmger Number I 3 I 4 I s 6 Initial Volume of liquid (H20) in impingers, (ml) drop out I 1 oo I 1oo I so Final (g) -------+------~------~-----+------4-------lnitial (g) -------+------4-----~~-----+------+------­Net (g) ============~=====d~====~=====k====== Total (g) =========== -r=== .r ,-.P' \s Plant'---:r:.f:C:....:..Gil.:....e.:.._,""l..:._"l-t----'---------Location~_5-----2Y~L __________ _ Analytical Method ____________ _ Do~~b Average Net Net Actual Net Net Gas ReadlnJ: Volume TestNo. • _ 2·~ 2·1 Gas Bag No. t -O.} Amb;~tT=p~ Operator I~· }(, ,v\ Date <tf / ;t...f /a; Average Net Actual Net Net Gas ReadinE Volume TestNo. "'2-G"BogNo.~ ~.0 ·'3·0 ).0 3·0 30 0 3·0 Ambient Temp Operator JSit, 1-Yb 1~------~----~1~----~r-----~lr-------T-----~I Average Net Date -----Test No.------ Gas Bag No.------ Ambient Temp------ Operator _____ _ Gas 0 1 (Net is Actual 0 2 Nel Actual Reading •o2 was determined using a gas analyzer CO is not measured, as it has the same molecular weight as N2 Net Volume Dryer Baghouse . Facility: Energy fuels Date: B{z"L/ 2oll, Stack Identification: Yellow Cake Dryer Baghouse X ('7'<'\2.L.b ~(....- lMPINGERS Filter Number: (...lo ... l IMPINGERS Filter Number: (..1 0 (q IMPING.EftS Filter Number: Final (g) Initial (g) Net (g) Final (g) Initial (g) Net (g) Run: l Sample Box: E llllpinger Number 2 I 3 I 4 I s 6 Initial Volume of liquid (H20) in impingers, (ml) 1 oo 1 oo I I sa I I ' l • • • lOB -) \..t(.-o {1"1· t 41 '1-'-l 7JD.o (,II.:) 51~.'1 ,OLf,.:, -L'( l.f '.1.-n.tJ Total (g) ======= Run: Sample Box: [ tnlpmger Number 1 I 3 I 4 I s 6 2 Initial Volume of liquid (H20) in impingers, (ml) I 00 1 00 I I sa I ' "ryj.y 7o'S. { -~ . ".-\' Run: 1 1 ' . lo s~.o .s-zo. z. Cj 1-5': 1.- ~ t \ ·0 j I "1. I 9t1,'-( })-0 {1. \ <;5-~ c::;,;-( ~ . ~ l/ Total (g) u Lf ========== • Sample Box: lmpmger Number 2 I 3 I 4 I 5 Initial Volume of liquid (H20) in impingers, (ml) 1 00 I 00 I I SG I • 6 Final (g)----t----+-----1-----l---~---­ Initial (g) ----1----+---4----+---~-----Net(g) ======~========================= Total (g) ======== fJ(z3/7.ol[p &r:zrz,'( l •' SDG No. Order No. ' ---- 52115 TestAmerica Inc rptSTLRcbTitle v3.73 TestAmerica Laboratories, Inc. Analytical Data Package Prepared For Denison Mines (USA) Corp. Radiochemical Analysis By TestAmerica Inc 2800 G.W. Way, Richland Wa, 99354, (509)-375-3131. Assigned Laboratory Code: Data Package Contains 23 Pages Report No.: 69831 Result~ in this report relate only to tbe sample(s) analyzed. Client Sample ID (List Order) Lot-Sa No. Work Order Report DB ID Batch No. .. -. -----·--R1 Dryer BH filter and J61130414-1 MB77P1AC 9MB77P10 6258020 beaker R1 Dryer BH filter and J61130414-1 M877P1AF 9M877P10 6258021 beaker R1 Dryer BH filter and J61130414-1 M877P1AE 9M877P10 6258022 beaker R1 Dryer BH filter and J61130414-1 M877P1AA 9M877P10 6258023 beaker R1 Dryer BH filter and J61130414-1 M877P1AD 9M877P10 6258024 beaker R1 Grizzly Baghouse filter J61130414-4 M878C1AC 9M878C10 6258020 and R1 Griuly Baghouse filter J61130414-4 M878C1AF 9M878C10 6258021 and R1 Grizzly Baghouse filter J61130414-4 M878C1AE 9M878C10 6258022 and R1 Grizzly Baghouse filter J61130414-4 M878C1AA 9M878C10 6258023 and R1 Grizzly Baghouse filter J61130414-4 M878C1AD 9M878C10 6258024 and R1 SYC Scrubber filter J61130414-2 M87741AC 9M877410 6258020 and bea R1 SYC Scrubber filter J61130414-2 M87741AF 9M877410 6258021 and bea R1 SYC Scrubber filter J61130414-2 M87741AE 9M877410 6258022 and bea R1 SYC Scrubber filter J61130414-2 M87741AA 9M877410 6258023 and bea R1 SYC Scrubber filter J61130414-2 MB7741AD 9M877410 6258024 and bea SDG No. Order No. 52115 TestAmeriCJI Inc rptSTLR.c:bTitle v3.73 \ TestAmerica Laboratories, Inc. t., Report No.: 69831 Results in this report relate only to the sample(s) analyzed. Client Sample ID (List Order} Lot-Sa No. Work Order Report DB ID Batch No. R2 SYC Scrubber filter J61130414-3 M87791AC 9M877910 6258020 and baa R2 SYC Scrubber filter J61130414-3 M87791AF 9M877910 6258021 and baa R2 SYC Scrubber filter J61130414-3 M87791AE 9M877910 6258022 and bea R2 SYC Scrubber filter J61130414-3 M87791AA 9M877910 6258023 and bea R2 SYC Scrubber filter J61130414-3 M87791AD 9M877910 6258024 and bea 2 Test America THE LEIIOER tN ENVIRONMENTAL TESTtNG Certificate of Analysis November 30, 2016 Denison Mines (USA) Corp 1 050 17th Street, Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab Project Name Sample Type SDGNumber I. Introduction September 9, 2016 Energy Fuels 2016 3rd Quarter Four (4) Stack Filter Samples 52115 CASE NARRATIVE On September 9, 2016, four stack filter samples were received at TestAmerica's Richland laboratory for radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification numbers as described on the cover page of the Analytical Data Package report form. The samples were assigned to Lot Numbers 161130414. II. Sample Receipt The samples were received in good condition and no anomalies were noted during check-in. III. Analytical Results/Methodology The analytical results for th:s report are presented by laboratory sample 10. Each set of data includes sample identification inform?tion; analytical results and the appropriate associated statistical uncertainties. The analysis requested was: TestAmerica Laboratories, Inc. Alpha Spectroscopy Th.o:i.um-228, -230, -232 by method RL-ALP-001 Uranium-234, -235, -238 by method RL-ALP-004 Gas Proportional Counting Pb-21 0 by method RL-GPC-0 II Radium-228 by method RL-RA-001 Alpha Scintillation Radium-226 by method RL-RA-001 3 Denison Mines (USA) Corp November 30, 2016 IV. Quality Control The analytical result for each analysis performed includes a minimum of one laboratory control sample (LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments" section. V. Comments Alpha Spectroscopy Thorium-228. 230, 232: The MDA for the samples and QC exceeds the CRDL due to method and matrix limitations. The blank activity for Th-230 is above the achieved MDA. The achieved MDA of the batch exceeds the detection limit due to reduced aliquot sizes taken due to historical process knowledge. There is no sample volume available for re-analysis. Data is reported. Except as noted, the LCS, batch blank and sample results are within acceptance criteria. Uranjum-234, 235, 238: Due to an analyst error, the uranium tracer was not added to the samples. There is no more volume available for re-analysis. The data was calculated using 100% for the tracer yield. The achieved MDA exceeds CRDL for all samples in this batch; the activity of the samples exceed the CRDL. Except as noted, the LCS, batch blank and sample results are within acceptance limits. Gas Proportional Counting Pb-210: The achieved MDA in the batch exceeds the CRDL due to method limitations for the matrix. The tracer yields and LCS recovery meet acceptance criteria. The sample results show no indication of met~od contribution. The blank activity exceeds the achieved MDA and CRDL, but is lower than sample and LCS activity; recqunt con finned. There is no sample volume remaining for re-analysis. Except as noted, the LCS, batch blank and sample results are within acceptance criteria. Radium-228: The achieved MDA in the batch exceeds the CRDL due to method limitations for the matrix. The tracer yields and LCS recovery rrieet acceptance criteria The sample results show no indication of method contribution. Data is reported. Except as noted, the LCS, batch blank and sample results are within acceptance limits. Alpha Scintillation Radium-226: The MDA for the samples and QC exceeds the CRDL due to method and matrix limitations. The blank activity is less than the achieved MDA. The LCS recovery is below acceptance criteria; recount confirmed. There is no sample volume available for re-analysis. Data is reported. Except as noted, the LCS, batch blank and sample results are within acceptance criteria. TestAmerica Laboratories, Inc. 4 Denison Mines (USA) Corp November 30, 20! 6 I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically and for completeness, for oth~r than the conditions detailed above. The Laboratory Manager or a designee, as verified by the following signature has authorized release of the data contained in this hard copy data package. Reviewed and approved: Erika Jordan (,~~2016.11.30 17:35:35 -os·oo· Erika Jordan Manager of Project Management TestAmerica Laboratories, Inc. 5 Drinking Water Method Cross References ---·--· ·-I ---DRINKING WAlER ASTM METHOD CROSS REFERENCES Referenced Method lsotope(s) TestAmerica Richland's SOP No. EPA 901.1 Cs-134, 1-131 RL-GAM-001 EPA 900.0 Alpha & Beta RL-GPC-001 EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002 EPA 903.0 Total Alpha Radium (Ra-226} RL-RA-002 EPA 903.1 Ra-226 RL-RA-001 EPA 904.0 Ra-228 RL-RA-001 EPA 905.0 Sr-89/90 RL-GPC-003 ASTM D5174 Uranium RL-KPA-003 EPA 906.0 Tritium RL-LSC-005 i I -·-··----· 1------·-----l -- Results in this report relate only to the sample(s) analyzed. Uncertainty Estimation TestAmerica Richland has adopted the internationally accepted approach to estimating uncertainties described in "NIST Technical Note 1297, 1994 Edition". The approach, "Law of Propagation of Errors", involves the identification of all variables in an analytical method which are used to derive a result. These variables are related to the analytical result (R) by some functional relationship, R == constants * f(x,y,z, ... ). The components (x,y,z) are evaluated to determine their contribution to the overall method uncertainty. The individual component uncertainties (ui) are then combined using a statistical model that provides the most probable overall uncertainty value. All component uncertainties are categorized as type A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the components, such as sample homogeneity, are combined with the component uncertainty as the square root of the sum-of-the-squares of the inrJividual uncertainties. The uncertainty associated with the derived result is the combined uncertajnty (uc) multiplied by the coverage factor (I ,2, or 3). When three or more sample replicates are used to derive the analytical result, the type A uncertainty is the standard deviation of the mean value (S/?n), where S is the standard deviation ofthe derived results. The type B uncertainties are all other random or non-random components that are not included in the standard deviation, The derivation of the general "Law of Propagation of Errors" equations and specific example are available on request. TestAmer1ca Inc rptGenerallnfo v3. 72 TestAmerica Laboratories, Inc. 6 . - ·-- --- I I L Action Lev Batch Bias COCNo Count Error (#s) CSll (#s) Uc Combined Standard Uncert. (#s), Coverage Factor CRDL(RL) Lc Lot-Sample No MDCIMDAIMDL Primary Detector Ratio U-234/U-238 Rst/MDC Rstffotllcert Report DB No RER SDG Sum Rpt Alpba Spec Rst(s) Work Order Yield TestAmerica Inc rptGeneranoro "3.72 TestAmerica Laboratories, Inc. Report Definitions An agreed upon activity level used to trigger some action when the final result is greater than or equal to the Action Level. Often the Action Level is related to the Decision Limit. The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed together. Defined by th.: equation (Result/Expected)-! as defined by ANSI Nl3.30. Chain of Custody Number assigned by the Client or TestAmerica. Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same units as the resuH. For Liquid Scintillation Counting (LSC) the batch blank count is the background. All known uncertainties associated with the preparation and analysis of the sample are propagated to give a measure of the uncertainty associated with the result, u" the combined standard uncertainty. The uncertainty is absolute and in the same units as the result. The coverage factor defines the width of the confidence interval, I, 2 or 3 standard deviations. Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmerica "default" nominal detection limit. Often refP,rred to the reporting level (RL) Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume associated with the sample. The Type I error probability is approximately 5%. Lc=( 1.645 • Sqrt(2"'(8kgmdCnt/BkgmdCnLMin)/SCntMin)) • (ConvFcti(Eff*Yid*Abn"'Vol) • lngrFct). For LSC methods the batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count is zero. The number assigned by the LIMS software to track samples received on the same day for a given client. The sample number is a sequential number assigned to each sample in the Lot. Detection Level based on instrument background or blank, adjusted by the Efficiency. Chemical Yield, and Volume with a Type I and II error probability of approximately 5%. MDC= (4.65 • Sqrt((Bkgrndl~nt!BkgrndCntMin)/SCntMin) + 2.71/SCntMin) • (ConvFct/(Eff • Yld • Abn • Vol} • lngrFct). For LSC methods the batch blank is used as a measure of the background variability. The instrument identifier associated with the analysis of the sample aliquot. The U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural uranium in NlST SRM 4321 C is 1.038. Ratio of the f<.:sult to the MDC. A value greater than l may indicate activity above background at a high level of confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of2 a value greater than I may indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order Number. The equation Replicate Error Ratio= (S-D)/(sqrt(TPUs2 + TPUd2)] as defined by lCPT BOA where S is the original sample result, Dis the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the total uncertainty of the duplicate sample. Sample Delive')' Group Number assigned by the Client or assigned by TestAmerica upon sample receipt. The sum ofthr. reported alpha spec results for tests derived ftom the same sample excluding duplicate result where the results are in the same units. The LIMS software assign test specific identifier. The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method. 7 Sample Results Summary Date: 30-Nov-16 TestAmerica Inc Ordered by Method, Batch No., Client Sample 10. Report No. : 69831 SDG No: 52115 Client ld Tracer Batch Wort< Order Parameter Result+-CSU ( 2 s) Qual Units Yield MDL CRDL RER2 6258023 RICHRC5011 R1 Dryer BH filter and beaker M877P1AA TH-228 -5.24E-09 +-1.5E-08 u uCi/Sample 22% 4.25E-08 TH-230 2.40E-07 +-1.2E-07 uCi/Sample 22% 4.50E-08 3.00E-15 TH-232 1.11 E-08 +-2.4E-08 u uCi/Sample 22% 4.50E-08 R1 Grizzly Baghouse filter and M878C1AA TH-228 7.80E-09 +-1.2E-08 u uCi!Sample 50% 2.02E-08 TH-230 2.63E-06 +-1.1 E-06 uCi/Sample 50% 1.91 E-08 3.00E-15 TH-232 2.95E-08 +-2.2E-08 uCi/Sample 50% 1.71 E-08 R1 SYC Scrubber filter and bea M87741AA TH-228 1.81 E-08 +-2.8E-08 u uCi/Sample 20% 4.71E-08 TH-230 1.89E-07 +-1.0E-07 uCi/Sample 20% 4.45E-08 3.00E-15 TH-232 1.10E-08 +-2.3E-08 u uCi/Sample 20% 4.45E-08 R2 SYC Scrubber filter and bea M87791AA TH-228 3.23E-08 +-2.2E-08 uCi/Sample 78% 1.70E-08 TH-230 3.39E-06 +-1.4E-06 uCi/Sample 78% 1.21E-08 3.00E-15 TH-232 9.22E-08 +-4.7E-08 uCi/Sample 78% 1.21 E-08 6258024 FFSR R1 Dryer BH filter and beaker M877P1AD U-234 4.27E-03 +-1.3E+OO uCi/Sample 100% 4.24E-05 9.00E-15 U-235 9.19E-05 +-2.8E-02 uCi/Sample 100% 4.24E-05 9.00E-15 U-238 4.42E-03 +-1.4E+OO uCi/Sample 100% 4.24E-05 9.00E-15 R1 Grizzly Baghouse filter and M878C1AD U-234 7.84E-05 +-2.8E-02 uCi/Sample 100% 5.23E-05 9.00E-15 U-235 -5.30E-07 +-1.9E-04 u uCi/Sample 100% 4.86E-05 9.00E-15 U-238 7.95E-05 +-2.8E-02 uCi/Sample 100% 4.86E-05 9.00E-15 R1 SYC Scrubber filter and bea M87741AD U-234 1.04E-03 +-3.6E-01 uCi/Sample 100% 5.15E-05 9.00E-15 U-235 1.30E-05 +-4.5E-03 u uCi/Sample 100% 4.79E-05 9.00E-15 U-238 1.16E-03 +-4.0E-01 uCi/Sample 100% 4.79E-05 S.OOE-15 R2 SYC Scrubber filter and bea M87791AD U-234 2.20E-03 +-8.0E-01 uCi/Sample 100% 5.79E-05 9.00E-15 U-235 4.06E-05 +-1.5E-02 u uCi/Sample 100% 5.49E-05 9.00E-15 U-238 1.77E-03 +-6.4E-01 uCi/Sample 100% 5.79E-05 9.00E-15 6258020 RICHRC5011 R1 Dryer BH filter and beaker MB77P1AC Pb-210 1.88E-05 +-7.5E-06 uCi/Sample 44% 7.18E-07 6.00E-14 R1 Grizzly Baghouse filter and M878C1AC Pb-210 3.37E-06 +-1.4E-06 uCi/Sample 84% 3.78E-07 6.00E-14 TestAmerlca Inc RER2 -Replicate Error Ratio = (S.D)/Isqrt(sq(TPUs)+sq(TPUd))l as defined by ICPT BOA. rptTALRchSaSum U Qual-Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncert, RDL or not identified by gamma scan mary2 V5.6 A2002 software. TestAmerica Laboratories, Inc. 8 Sample Results Summary Date: 30-Nov-16 TestAmerica Inc Ordered by Method, Batch No., Client Sample ID. Report No. : 69831 SDG No: 52115 Client ld Tracer Batch Wort Order Parameter Result+· CSU ( 2 s) Qual Units Yield MDL CRDL 6258020 RICHRC5011 R1 SYC Scrubber filter and bea MB7741AC Pb-210 5.34E-06 +-2.2E-06 uCi/Sample 47% 6.98E-07 6.00E-14 R2 SYC Scrubber filter and bea M87791AC Pb-210 1.42E-05 +-5.7E-06 uCi/Sample 67% 4.46E-07 6.00E-14 6258021 BRTF R1 Dryer BH filter and beaker M877P1AF Ra-228 4.59E-06 +-1.7E-06 uCi/Sample 21% 2.38E-06 9.00E-14 R1 Grizzly Baghouse filter and M878C1AF Ra-228 2.04E-06 +-5.6E-07 uCi/Sample 83% 7.07E-07 9.00E-14 R1 SYC Scrubber filter and bea M87741AF Ra-228 2.77E-06 +-1.2E-06 uCi/Sample 26% 1.63E-06 9.00E-14 R2 SYC Scrubber filter and bea M87791AF Ra-228 2.45E·06 +-7.1 E-07 uCi/Sample 55% 8.89E-07 9.00E-14 6258022 BRTE R1 Dryer BH filter and beaker M877P1AE Ra-226 2.87E-07 +-3.1E-07 u uCi/sample 23% 4.74E-07 9.00E-14 R1 Grizzly Baghouse filter and M878C1AE Ra-226 4.07E-06 +-1.8E-06 uCi/sample 100% 8.45E-08 9.00E-14 R1 SYC Scrubber filter and bea M87741AE Ra-226 1.86E-07 +-2.1 E-07 u uCi/sample 29% 3.23E-07 9.00E-14 R2 SYC Scrubber filter and bea M87791AE Ra-226 5.60E-06 +-2.5E-06 uCi/sample 64% 1.56E-07 9.00E-14 No. of Results: 36 TestAmerfca Inc RER2 -Replicate Error Ratio= (S-D)/Jsqrt(sq(TPUs}tsq(TPUd))l as defined by ICPT BOA. rptT ALRchSaSum mary2 V5.8 A2002 U Qual -Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncert, RDL or not identified by gamma scan software. TestAmerica Laboratories, Inc. 9 RER2 QC Results Summary Date: 30-Nov-16 TestAmerica Inc Ordered by Method, Batch No, QC Type,. Report No. : 69831 SDG No.: 52115 Batch Tracer LCS Work Order Parameter Result+-CSU ( 2 s) Qual Units Yield Recovery Bias MDL RICHRCS011 6258023 BLANK QC, M87981AA TH-228 -9.03E-09 +-1.8E-08 u Ci/Sample 23% 5.83E-08 TH-230 3.41 E-08 +-3.1 E-08 Ci/Sample 23% 3.33E-08 TH-232 -9. 75E-09 +-1.6E-08 u Ci/Sample 23% 4.83E-08 6258023 LCS, M87981AC TH-230 9.64E-09 +-1.6E-09 Ci/Sample 43% 85% -0.1 1.10E-10 FFSR 6258024 BLANK QC, M87991AA U-234 2.63E-08 +-3.9E-08 u Ci/Sample 101% 5.41 E-08 U-235 O.OOE+OO +-2.7E-08 u Ci/Sample 101% 5.03E-08 U-238 -5.48E-10 +-2.7E-OB u Ci/Sample 101% 5.03E-08 6258024 LCS, MB7991AC U-234 3.32E-06 +-7.2E-07 Ci/Sample 97% 101% 0.0 5.36E-08 U-238 3. 15E -06 +-6. 9E-07 Ci/Sample 97% 92% -0.1 5.36E-OB RICHRCS011 6258020 BLANK QC, M87951AA Pb-210 6.10E-07 +-2.4E-07 Ci/Sample 85% 3.36E-07 6258020 LCS, M87951AC Pb-210 1.01 E-05 +-1.8E-06 Ci/Sample 90% 112% 0.1 3.38E-07 BRTF 6258021 BLANK QC, M87961AA Ra-228 1.35E-06 +-4.3E-07 Ci/Sample 86% 5.76E-07 6258021 LCS, M87961AC Ra-228 1.27E-05 +-1. 7E-06 Ci/Sample 79% 124% 0.2 7.25E-07 BRTE 6258022 BLANK QC, M87971AA Ra-226 2.92E-08 +-3.9E-08 u Ci/sample 100% p.34E-08 6258022 LCS, M87971AC Ra-226 9.05E-06 +-1.8E-06 Ci/sample 88% 91% -0.1 9.32E-08 No. of Results: 15 TestAmerica Inc Bias -(Result/Expecred)-las defined by ANSI N13.30. rptSTLRchQcSum U Qual-Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncert, RDL or not identified by gamma scan software. mary V5.8 A2002 Tes!America Laborator1es, Inc. 10 FORM I Date: 30-Nov-16 SAMPLE RESULTS Lab Name: TestAmerica Inc SDG: 52115 Collection Date: 8/22/2016 1:00:00 PM Lot-sample No.: J61130414-1 Report No.: 69831 Received Date: 9/9/2016 11:35:00 AM Client Sample ID: R1 Dryer BH filter and beaker CCC No.: Matrix: SOLID Ordered b~ Client Samele ID, Batch No. Count csu MDL, Rpt Unit, Yield Rst/MDL, Analysis, Parameter Result Qual Error ( 2 s) (2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Prep Date B'lltch: l.i258020 RICHRC5011 ii'VIlr!( Order: M87i P1AC Report DB ID: 9M877PHl Pb-2.10 1.88E-05 8.4E-07 7.5E-06 7 .18E-07 uCi/Sample 44% (26.2) 10/25/1611:54 a 3.49E-07 6.00E-14 (5.) Batch: 6258021 BRTF Work Order: M877P1AF Report DB ID: 9MB77P10 Ra-2.28 4.59E-06 1.6E-06 1.7E-06 2.38E-06 uCi/Sample 21% (1.9) 11/29/16 03:11 p 1.03E-06 9.00E-14 (5.3) Batch: 6258022 BRTE Work Order: M877P1AE Report DB ID: 9M877P1 0 Ra-226 2.87E-07 u 2.9E-07 3.1E-07 4.74E-07 uCi/sample 23% 0.61 11/18/16 07:49 p 2.29E-07 9.00E-14 (1 .8) Batch: 6258023 RICHRC5011 Work Order: MB77P1AA Report DB ID: 9M877P10 TH-228 -5.24E-09 U 1.5E-08 1.5E-OB 4.25E-08 uCi/Sample 22% -0.12 10/19/16 01:56 a 1.71E-OB -0.69 TH-230 2.40E-07 7.9E-08 1.2E-07 4.50E-08 uCi/Sample 22% (5.3) 10/19/16 01 :56 a 1.84E-08 3.00E-15 (3.9) TH-232 1.11E-08 u 2.3E-08 2.4E-08 4.50E-08 uCi/Sample 22% 0.25 10/19/16 01 :56 a 1.84E-OB 0.95 Batch: 6258024 FFSR Work Order: M877P1AD Report DB ID: 9M877P10 U-234 4 .27E-03 4.4E-04 1.3E+OO 4 .24E-05 uCi/Sample 100% (100.8) 10/1 B/16 06:29 p 3.87E-06 9.00E-15 0.01 U-235 9.19E-05 6.5E-05 2.8E-02 4.24E-05 uCi/Sample 100% (2.2) 10/18/16 06:29 p 3.87E-06 9.00E-15 0.01 TastAmerlca Inc MDCIMDA,Lc -Detection, Decision Level based on Instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria, Mdc/MdaiMdl, Total Uncert, RDL or not Identified by gamma scan software. V6.8 A2002 TestAmerica Laboratories, Inc. 11 Total Sa Aliquot Primary Size Size Detector 1.0 0.96874 GPC31B Sample Sample 1.0 0.96874 GPC4C Sample Sample 1.0 0.9687 ASC5UC Sample Sample 1.0 0.96874 ALP128 Sample Sample 1.0 0.96874 ALP128 Sample Sample 1.0 0.96874 ALP128 Sample Sample 'to 0.00112 ALP411 Sample Sample 1.0 0.00112 ALP411 Sample Sample '- FORM I SAMPLE RESULTS Date: 30-Nov-16 Lab Name: TestAmerlca Inc Lot~ample No.: J61130414-1 Client Sample ID: R1 Dryer BH filter and beaker SDG: 52115 Report No. : 69831 COC No.: Collection Date: B/22/2016 1 :00:00 PM Received Date: 9/9/2016 11:35:00 AM Matrix: SOLID Ordered by Client Sample I D. Batch No. Count csu MDL, Rpl Unit, Yield RsUMDL, Analysis, Parameter Result Qual Error ( 2s) (2 8) Action Lev Lc CRDL(RL) RsUTotUcert Prep Data U-238 4.42E-03 4.5E-D4 1.4E+OO 4.24E-Q5 uCIISample 100% (104.3) 10/18/16 06:29 p 3.87E-06 9.00E-15 0.01 Ratio U.234123B = 1.0 No. of Results: 9 Comments: ,• .. .. TestAmerlca Inc MDCIMDA,Lc -Detection, Decision Level basad on Instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual-Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncart, RDL or not Identified by gamma scan software. V6.8 A2002 Tes!America Laboratories, Inc. 12 Total Sa Aliquot Primary Size Size Detector 1.0 o.oom ALP411 Sample Sample FORM I Date: 30-Nov-16 SAMPLE RESULTS Lab Name: TestAmerica Inc SDG: 52115 Collection Date: 8/23/2016 9:00:00 AM Lot-Sample No.: J61130414-4 Report No.: 69831 Received Date: 9/9/2016 11:35:00 AM Client Sample ID: R1 Grizzly Baghouse filter and coc No.: Matrix: SOLID Ordered b~ Client Samele ID, Batch No .• Count csu MDL, Rpt Unit, Yield Rst/MDL, Analysis, Parameter Result Qual Error ( 2 a) (2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Prep Date Batch: 62580~0 RICHRCSll!1 Work Order: M878C1AC Report DB ID: 9M878Clll Pb-210 3.37E-06 3.1 E-07 1.4E-06 3.78E-07 uCi/Sample 84% (8.9) 10/25/1611:55 a 1.83E-07 B.OOE-14 (4.9) Batch: 6258021 BRTF Work Order: M878C1AF Report DB ID: 9M878C10 Ra-228 2.04E-06 5.1E-07 5.6E-07 7.07E-07 uCi/Sample 83% (2.9) 11/29/16 03:12 p 3.19E-07 9.00E-14 (7.4) Batch: 6258022 BRTE Work Order: M878C1AE Report DB ID: 9M878C10 Ra-226 4.07E-06 1.4E-07 1.8E-06 8.45E-08 uCilsample 100% (48.2) 11/18/16 07:49 p 4.07E-08 9.00E-14 (4.6) Batch: 6258023 RICHRC5011 Work Order: M87BC1AA Report DB ID: 9M878C10 TH-228 7.80E-09 u 1.2E-08 1.2E-08 2.02E-08 uCi/Sample 50% 0.39 10/19116 01 :57 a 8.29E-09 (1.3) TH-230 2.63E-06 1.7E-07 1.1 E-06 1.91 E-08 uCi/Sample 50% (137.5) 10/19/16 01 :57 a 7.84E-09 3.00E-15 (5.) TH-232 2.95E-08 1.8E-08 2.2E-08 1.71E-08 uCi/Sample 50% (1. 7) 10/19/16 01 :57 a 6.88E-09 (2.7) Batch: 6258024 FFSR Work Order: M87BC1AD Report DB ID: 9M87BC10 U-234 7.84E-05 6.5E-05 2.8E-02 5.23E-05 uCi/Sample 100% (1.5) 10/18/16 06:31 p 6.29E-06 9.00E-15 0.01 U-235 -5.30E-07 U 2.7E-05 1.9E-04 4.86E-05 uCi/Sample 100% -0.01 10/18/16 06:31 p 4.44E-06 9.00E-15 -0.01 TestAmerlca Inc MDCIMDA,Lc • Detection, Decision Level based on Instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual-Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncert, RDL or not Identified by gamma scan software. V6.8A2002 Tes!America Laboratories, Inc. 13 Total Sa Aliquot Primary Size Size Detector 1.0 0.95786 GPC32A Sample Sample 1.0 0.95786 GPC6B Sample Sample 1.0 0.9579 ASCKAB Sample Sample 1.0 0.95786 ALP131 Sample Sample 1.0 0.95786 ALP131 Sample Sample 1.0 0.95786 ALP131 Sample Sample 1.0 0.00098 ALP434 Sample Sample 1.0 0.00098 ALP434 Sample Sample FORM I SAMPLE RESULTS Date: 30-Nov-16 Lab Name: TestAmerica Inc Lot-Sample No.: J61130414-4 Client Sample ID: R1 Grizzly Baghouse filter and SDG: 52115 Report No.: 69831 COC No.: Collection Date: 8/23/2016 9:00 :00 AM Received Date: 9/9/2016 11 :35:00 AM Matrix: SOLID Ordered by Client Sample ID, Batch No. Count csu MDL, Rpt Unit, Yield Rst/MDL, Analysis, Parameter Result Qual Error ( 2 s) (2 B) Action Lev Lc CRDL(RL) RstJTotUcart Prep Data U-23-~ 7.95E-05 6.5E-05 2.8E-O? 4.86E-05 uCi/Sample 100% (1.6) '10/18/16 OR:31 p 4.44E-06 9.00E-15 0.01 Ratto U-2341238 = 1.0 No. of Results: 9 Comments: TeatAmartca Inc MDCIMDA,Lc-Detection, Decision Level based on Instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncart, RDL or not ldentmad by gamma scan software. Vli.S A2002 TestAmerica Laboratories, Inc. 14 Total Sa Aliquot Primary Size Size Detector 1.0 0.00098 ALP434 Sample Sample FORM I Date: 30-Nov-16 SAMPLE RESULTS Lab Name: TestAmerica Inc SDG: 52115 Collection Date: 8/23/2016 8:00:00 AM Lot-Sample No.: J61130414-2 Report No.: 69831 Received Date: 9/9/2016 11:35:00 AM Client Sample 10: R1 SYC Scrubber filter and bea COC No.: Matrix: SOLID Ordered b~ Client Samele ID. Batch No. Count csu MDL, Rpt Unit, Yield Rst/MDL, Analysis, Total Sa Aliquot Primary Parameter Result Qual Error( 2•1 (2 s) Action Lev lc CRDL(RL) Rst/TotUcert Prep Date Size Size Detector aatch: 62580 .. () RICHRC501 I Work Ord&r: M87741AC Report lli::IID: 9M877.t10 Pb-210 5.34E-06 5.6E-07 2.2E-06 6.98E-07 uCi/Sample 47% (7.6) 10/25/16 11 :54 a 1.0 0.95547 GPC31C 3.39E-07 6.00E-14 (4.8) Sample Sample Batch: 6258021 BRTF Work Order: M87741AF Report DB ID: 9M877410 Ra-228 2.77E-06 1.1E-06 1.2E-06 1.63E-06 uCi/Sample 26% (1 . 7) 11/29/1603:11 p 1.0 0.95547 GPC4D 6.86E-07 9.00E-14 (4.7) Sample Sample Batch: 6258022 BRTE Work Order: M87741AE Report DB 10: 9M877410 Ra-226 1.86E-07 u 2.0E-07 2.1E-07 3.23E-07 uCi/sample 29% 0.58 11/18/16 07:49 p 1.0 0.9555 ASCDUE 1.56E-07 9.00E-14 (1.8) Sample Sample Batch: 6258023 RICHRC5011 Work Order: M87741AA Report DB 10: 9M877410 TH-228 1.81E-08 u 2.7E-08 2.8E-08 4. 71 E-08 uCi/Sample 20% 0.39 10/19/1601:56a 1.0 0.95547 ALP129 1.93E-08 (1.3) Sample Sample TH-230 1.89E-07 7.0E-08 1.0E..07 4.45E-OB uCi/Sample 20% (4.2) 10/19/16 01 :56 a 1.0 0.95547 ALP129 1.82E-OB 3.00E-15 (3.6) Sample Sample TH-232 1.10E-OB u 2.3E-OB 2.3E-08 4.45E-06 uCi/Sample 20% 0.25 10/19/16 01 :56 a 1.0 0.95547 ALP129 1.82E-OB 0.95 Sample Sample Batch: 6258024 FFSR Work Order: M87741AD Report DB ID: 9M877410 U-234 1.04E-03 2.3E-04 3.6E-01 5.15E-05 uCi/Sample 100% (20.2) 10/1 B/16 06:30 p 1.0 0.001 ALP412 6.1BE-06 9.00E-15 0.01 Sample Sample U-235 1.30E-05 u 2.6E-05 4.5E-03 4.79E-05 uCi/Sample 100% 0.27 10/18/16 06:30 p 1.0 0.001 ALP412 4.37E-06 9.00E-15 0.01 Sample Sample TestAmerlcalnc MDCIMDA,lc ·Detection, Decision Level baaed on Instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria, MdciMda/Mdl, Total Uncert, RDL or not Identified by gamma scan software. V6.8 A2002 TesiAmerlca Laboratories, Inc. 15 FORM I SAMPLE RESULTS Date: 30-Nov-16 Lab Name: TestAmerica Inc Lot-Sample No.: J61130414-2 Client Sample 10: R1 SYC Scrubber filter and bea SDG: 52115 Report No.: 69831 COC No.: Collection Date: 8/23/2016 8:00:00 AM Received Date: 9/9/2016 11:35:00 AM Matrix: SOLID Ordered by Client Sample ID, Batch No. Count csu MDL, Rpt Unit, Yield Rst/MDL, Analysis, Parameter Result Qual Errorl2s1 12 s) Action Lev Lc CRDLjRL) RstiTotUcert Prep Date U-238 1.16E-03 2.5E-Od 4.0E-D1 4.79E-05 uCi/Sample 100% (24.2) 10/18/16 C6:30 p 4.37E-06 9.00E-15 0.01 Rstlo U-2341238 = 0.9 No. of Results: 9 Comments: TestAmerlca Inc MDCIMDA,Lc • DetecUon, Decision Level based on Instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual· Analyzed for but not detected above llmiUng criteria, MdcJMdaiMdl, Total Uncert, RDL or not Identified by gamma scan software. V6.8A2002 TesiAmerica Laboratories, Inc. 16 Total Sa Aliquot Primary Size Size Detector 1.0 0.001 ALP412 Sample Sample .... I J I , I l I . ' lk. ,. I •I l l tl q ~i I I' I. [ !· .. FORM I Date: 30-Nov-16 SAMPLE RESULTS Lab Name: TestAmerica Inc SDG: 52115 Collection Date: 8/24/2016 12:00:00 PM Lot-Sample No.: J61130414-3 Report No.: 69831 Received Date: 9/9/2016 11:35:00 AM Client Sample 10: R2 SYC Scrubber filter and bea COC No.: Matrix: SOLID Ordered b.~ Client Sam~le I D. Batch No. Count csu MDL, Rpt Unit, Yield Rst/MDL, Analysis, Total Sa Aliquot Primary Parameter Result Qual Error ( 2•1 (2 s) Action Lev Lc CRDL(RL) RstlTotUcert Prep Data Size Size Detector &atch: 625802G RICHRC5011 Work Order: MB7791AC Report DB ID: 9MB7791 0 Pb-210 1.42E-05 5.7E-07 5.7E-06 4.46E-07 uCi/Sample 67% (31.9) 10/25/16 11:54 a 1.0 0.95202 GPC31D 2.16E-07 6.00E-14 (5.) Sample Sample Batch: 6258021 BRTF Work Order: MB7791AF Report DB 10: 9M877910 Ra-228 2.45E-06 6.5E-07 7.1E-07 8.89E-07 uCi/Sample 55% (2.8) 11/29/16 03:12 p 1.0 0.95202 GPCSA 3.93E-07 9.00E-14 (6.9) Sample Sample Batch: 6258022 BRTE Work Order: M87791AE Report DB 10: 9M877910 Ra-226 5.60E-06 2.3E-07 2.5E-06 1.56E-07 uCi/sample 64% (35.9) 11/18/16 07:48 p 1.0 0.952 ASCHSB 7.52E-08 9.00E-14 (4.4) Sample Sample Batch: 6258023 RICHRC5011 Work Order: M87791M Report DB 10: 9M877910 TH-228 3.23E-08 1.8E-08 2.2E-08 1. 70E-08 uCi/Sample 78% (1.9) 10/19/16 01 :57 a 1.0 0.95202 ALP130 6.97E-09 (2.9) Sample Sample TH-230 3.39E-06 1.7E-07 1.4E-06 1.21 E-08 uCi/Sample 78% (280.) 10/19/16 01:57 a 1.0 0.95202 ALP130 4.79E-09 3.00E-15 (5.) Sample Sample TH-232 9.22E-08 2.9E-08 4.7E-08 1.21 E-08 uCi/Sample 78% (7.6) 10/19/16 01:57 a 1.0 0.95202 ALP130 4.79E-09 (4.) Sample Sample Batch: 6258024 FFSR Work Order: M87791AD Report DB ID: 9M877910 U-234 2.20E-03 3.5E-04 B.OE-01 5.79E-05 uCi/Sample 100% (37.9) 10/18/16 06:30 p 1.0 0.00095 ALP433 8.09E-06 9.00E-15 0.01 Sample Sample U-235 4.06E-05 u 4.8E-05 1.5E-02 5.49E-05 uCi/Sample 100% 0.74 10118/16 06:30 p• 1.0 0.00095 ALP433 6.60E-06 S.OOE-15 0.01 Sample Sample TestAmerlca Inc MDCIMDA,Lc-Detection, Decision Level based on Instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual-Analyzed for but not detected above limiting criteria, MdcJMdaiMdl, Total Uncert, RDL or not Identified by gamma scan software. V5.8 A2002 TestAmerica Laboratories. Inc. 17 Lab Name: TestAmerica Inc Lot-Sample No.: J61130414-3 Client Sample ID: R2 SYC Scrubber filter and bea Count csu Parameter Result Qual Error ( 2•1 (2 a) U-238 1.77E-03 3.1E-OI! 6.4E-01 No. of Results: 9 Comments: FORM I SAMPLE RESULTS SDG: 52115 Report No. : 69831 COC No.: MDL, Rpt Unit, Yield Rst/MDL, Action Lev Lc CRDL(RL) RstiTotUcert 5.79E-Q5 uCi/Sample 100% (30.5) B.09E-06 9.00E-15 0.01 Ratio U·234123B = 1.2 Date: 30-Nov-16 Collection Date: 8/24/2016 12:00:00 PM Received Date: 9/9/2016 11:35:00 AM Matrix: SOLID Ordered by Client Sample ID, Batch NG. Analysis, Total Sa Aliquot Primary Prep Date Size Size Detector 10/1 B/16 06:30 p 1.0 0.00095 ALP.433 Sample Sample TestAmerlca Inc MDCIMDA.Lc • Detection, Decision Level based on Instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTl.RchSample U Qual-Analyzed for but not detected above limiting criteria, MdcJMdaiMdl, Total Uncert, RDL or not Identified by gamma scan software. V6.8A2002 TestAmerica Laboratories, Inc. 18 -' J J FORM II Date: 30-Nov-16 BLANK RESULTS Lab Name: TestAmerica Inc SDG: 52115 Matrix: SOLID Report No.: 69831 Count csu . MDL, Rpt Unit, Rst/MDL, Analysis, Total Sa Aliquot Primary Parameter Result Qual Error ( 2 s) (2&) Lc CRDL Yield Rst/TotUcert Prep Date Size Size Detector Batch: 6258020 RICHRC5011 Work Order: M87951AA Report DB ID: M87951AB Pb-210 6.10E-07 2.2E-07 2.4E-07 3.36E-07 uCi/Sample 85% (1.8) 10/25/16 11:55 a 1.0 1.0 GPC328 1.63E-07 6.00E-14 (5.1) Sample Sample Batch: 6258022 BRTE Work Order: M87971AA Report DB ID: MB7971AB Ra-226 2.92E-08 u 3.8E-08 3.9E-08 6.34E-08 uCi/sample 100% 0.46 11/18/16 07:49 p 203.1 203.1 ASCMAD 3.03E-08 9.00E-14 (1.5) g g Batch: 6258021 BRTF Work Order: MB7961AA Report DB 10: M87961AB Ra-228 1.35E-06 4.0E-07 4.3E-07 5.76E-07 uCi/Sample 86% (2.3) 11/29/16 03:12 p 1.0 1.0 GPC6C 2.57E-07 9.00E-14 (6.2) Sample Sample Batch: 6258024 FFSR Work Order: M87991AA Report DB 10: M87991AB U-234 2.63E-08 u 3.9E-08 3.9E-08 5.41 E-08 uCifSample 101% 0.49 10/18/16 06:32 p 1.0 1.0 ALP435 1.15E-08 9.00E-15 (1.3) Sample Sample U-235 O.OOE+OO u O.OE+OO 2.7E-08 5.03E-OB uCi/Sample 101% 0. 1 0/18/16 06:32 p 1.0 1.0 ALP435 9.83E-09 9.00E-15 0. Sample Sample U-238 -5.48E-10 u 2.7E-08 2.7E-08 5.03E-08 uCi/Sample 101% -0.01 10/18/16 06:32 p to 1.0 ALP435 9.83E-09 9.00E-15 -0.04 Sample Sample Ratio U-2341238 = -48.0 Batch: 6258023 RICHRC5011 Work Order: M87981AA Report DB ID: M87981AB TH-228 -9.03E-09 u 1.8E-08 1.8E-08 5.83E-08 uCi/Sample 23% -0.16 10/19116 01 :59 a 1.0 1.0 ALP24 2.47E-08 -1 . Sample Sample TH-230 3.41E-08 3.0E-08 3.1E-08 3.33E-08 uCi/Sample 23% (1.) 10/19/16 01 :59 a 1.0 1.0 ALP24 1.32E-08 3.00E-15 (2.2) Sample Sample TestAmerlcalnc MDCIMDA,Lc -Detection, Decision Level based on Instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchBiank U Qual-ADal)-zed for but out detected above llmitlog criteria, MdcfMda/1\tdl, Total Uocert, RDL or oot idmtlfted by gamma scao software. V&.B A2002 Tes!America Laboratories, Inc. 19 Lab Name: TestAmerica Inc Matrix: SOLID Count csu Parameter Result Qual Error ( 2 &) (2 s) TH-232 -9.75E-09 u 1.6E-08 1.6E-08 No. of Results: 9 Comments: MDL, Lc FORM II BLANK RESULTS RptUnlt,. CRDL Yield 4.83E-08 uCi/Sample 23% 2.00E-08 Rst/MDL, Rat/TotUcert -0.2 -{1.2) _J SDG: 52115 Report No.: 69831 Analysis, Total Sa Prep Date Size 10/19/16 01 :59 a 1.0 Sample TestAmerlca Inc MDCIMDA,Lc • Detection, Decision Level based on Instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchBiank U Quad· Analyzed ror but oot detected above llndtlog criteria, Mdc/Mda/Mdl, Total Uucert, RDL or uot ideo tiDed by gam11111 scau sortware.. V&.B A2002 TestAmerica Laboratories, Inc. 20 Date: 30-Nov-16 Aliquot. Primary Size Detector 1.0 ALP24 Sample Lab Name: TestAmerica Inc Matrix: SOLID Parameter Batch: 6258020 Pb-210 Batch: 6258022 Ra-226 Batch: 6258021 Ra-228 Batch: 6258024 U-234 U-238 Batch: 6258023 TH-230 Result RICHRC5011 1.01 E-05 BRTE 9.05E-06 BRTF 1.27E-05 FFSR 3.32E-06 3.15E-06 RICHRC5011 9.64E-09 Count Qual Error ( 2 s) 4.1E-07 2.0E-07 9.0E-07 4.2E-07 4.1E-07 7.7E-10 -· FORM II LCS RESULTS SDG: 52115 Report No.: 69831 csu (2 s) Report Unit Expected' Recovery, Analysis, Prep Date MDL Yield Expected Uocert Bias Work Order: M87951AC Report DB ID: M87~51CS 1.8E-06 3.38E-07 uCi/Sample 90% 9.03E-OE' 1.54E-D7 11L% 10/25/16 11:55 a Rec Limits: 75 125 0.1 Work Order: M87971AC Report DB ID: M87971 CS 1.8E-06 9.32E-08 uCi/sample 88% 9.91 E-06 1.01 E-07 91% 11/18/16 07:49 p Rec Limits: 75 125 -0.1 Work Order: M87961AC Report DB ID: M87961CS 1. 7E-06 7 .25E-07 uCi/Sample 79% 1.02E-05 1.16E-07 124% 11/29/16 03:12 p Rec Limits: 75 125 0.2 Work Order: M87991AC Report DB ID: MB7991CS 7.2E-07 5.36E-08 uCi/Sample 97% 3.28E-06 1.73E-08 101% 10/1 8/16 09:26 p Rec Limits: 75 125 0.0 6.9E-07 5.36E-08 uCi/Sample 97% 3.44E-06 1.81 E-08 92% 10/18/16 09:26 p Rec Limits: 75 125 -0.1 Work Order: M87981AC Report DB ID: MB7981CS 1.6E-09 1.10E-10 uCi/Sample 43% 1.13E-08 1.1BE-10 85% 10/23/16 06:18 a Rec Limits: 75 125 -0.1 No. of Results: 6 ·----.. ------------·-·-·--Comments: TestAmerlca Inc Bla! • (Resuii/Expected)-1 as deHned by ANSI N13.30. rptSTLRchlcs V5.8 A2002 TestAmerica Laboratories, Inc. 21 Date: 30-Nov-16 Aliquot Primary Slza Detector 1.0 GPC32C Sample 200.54 ASCPMD g 1.0 GPC6D Sample 1.0 ALP436 Sample 1.0 ALP436 Sample 200.54 ALP128 Sample ~ Ul :;; 3 It :::lo &l r Ill cr 0 iii 0 ffio !!' 3" !1 N "' . , J. __ ., -. . ~ ~ ... CfiiliJ of Custody Record Temperature on Receipt --- ""S ~'S.-\ ::P'-\ '"-\ TestAmerica ~~-Sd-''5 ' TAL-'1~(11J)7) Gl!nl1 : Tetco j391 East 620 South Dt(nldng water? Yes 0 ° NoD THE LEADER IN ENVIRONMENTAl TESTING ; ~~ Dean Kltche n. i I f:o7/201£ /Jib Number .sool-4n-09.1Q6 _ • r.&akt ;:,/ Ct_.,., IJi.IMN, , o• ···----~---OJ Pt1ge I or 1 ~-:A'meri~~-~f~rk ,. l~j=--~unmav .1i6b~--I =~ I 'bellret•k"'""""'--~' ·---··o·o-" -~Numbtlr 0 L r-.L I I I I :Jflergy ~t!~ls ,1,01~ ~rd Qua.r!~r. . _ 0 _ .. __ J · 0 ; ;l ! 1 I ~ 01Tfs110uote No. . Contslners & 0 ; ~ o! Mlltrix 0 '"'1!1 l c:> :j; o Pt8t1eMIIivl!S • a; ~ 0 ~ ~ ~ 1:: "' j --~/61.0. folD. and0e$Crlpllon Dilts TltTI8 ~ "' ~ i ~ B -~ ~ili 0 ~ :: ~ l l ~I ~ J SpsciBI/nstrvctlonSI Cond/Uons of Receipt ~ /or nch41lf'11pla m4Y be~ 011 antl/inej ~ t 41 .. ! ~ f ~ f ~.! -1=1. ~' ~ r- 'Rl DryerSH filterandbeaker_ 0 -·--f o~!~l~'i.:~:.; 13:~~-_j ~) . ox.ll:t.J_tij~l '/ 1-f.. 11 T 1 T {'{l"'&'l~Q ~ Rl SYCScrubber fllter and beaker j i B/23/16 8:00 J lxJ o?CJlJWL~ '/.. 'f. )C ll l l _l If/\ 'fYl Y'\ '-\ l R2SYCSc:rubberf!lter andbeaker_ =::fs/24/16 !1 12:00 ii;J I I I I f I I I I I I iJtf,~:~-j)l..j 1-1~ I I I I I I '4\1'\<brP'\~ I Rl GrllzlyBaghouseFllterand Buker J l s/23!!~_.1 L9W _OJ IX I I I I I I I I I t I If-I)( I)\ IX I~ I xlx: I I I I I I >fV'\ 1l\.:t G r I I -• _ .... 0 ... -• ___ I Poss!liii 111iDn:t~ 0 Mln-HtiZifrf 0 FlllmmBb/8 0 Sldn JaUnt oPoGons -o~~~~Oin fum AIIMid Ttlltt Rffqlllied f. 2. 3.~ey ~ ! When Complete Email to: Dean or Paul tetco@tetco-ut.com lilfmliBOWiiC Wl'lfl'E· ~ G'WAF!l"~li«ii 5 Siiijllj; PINK -FWCJ~y D DJ.poui By Lab 0 Archfo;e F« Monfti4 (A frle t118Y ba Brlti«<SSJd if~ 1118 RIIBinsd ----~~1 ~) ~~!s(SpeciTy) ~ r ' o.jU DIUII IUI!IIIfilllfil J6130414 . ' ......... -· ··-·---- ------------·-o-0 Test America sample check-In Ltst THE LEAD.ER IN EHVIAONt.lt:NTAL TD8T1~ I Date/Time Received: \. ...... '\.-\ '-"' \\ '"!J S C~mtainer GM Screen Result: (Airlock) 0 ·-. Sample GM Screen Result (Sampl~ Receiving-)=0'---- Client: :\) ~ · SDG #: 5)~ \\ S Lot Number: ~ l..(s_ \ ":o_"-'._\ '-\--->..,.._ __ _ ., ChainofCustody#""'\:l~}'-1'~..__--------------------------·-----/ .. I 1 ' ·I 1i Shipping Container ID or Air Bill Number :----------..------ Samples received inside shipping container/cooler/box ~~~ ] Continue with 1 through 4. Initial appropriate response. ] Go to 5, add comment to #16. 1. Custody Seals on shipping container intact? 2. Custody Seals dated and signed? Yes[ Yes[ ] No [ No Custody Seal ~ ] ] No [ No ~stody Seal ~ J "C NA ] T _N_A _[-Wet[ ] Dry~] 3. Cooler temperature: 4. Vermiculite/packing materials is Item 5 through 16 for samples. Initial ;.,ppropriate response. ~- 5. Chain of Custody record preseo~? Yes ] No [ ] 6. Number of samples received (Each sample may contain mu iple bottles):._~-+--- 7. Containers received: \.\ ~ Q~ .. \W: ~ '{, aSO ~'-n -f' 'C' i -=\ . K" 8. 9. 10. 11. Sample holding times exceeded? NA [ Yes [ ] ~No 't ] S=plos ,, __ tape · __ hazard labels __ custody seals app;J;riate sample labels Matrix: A (FLT, Wipe, Solid, Soil) __ ,_l (Water) __ s (Air, Niosh 74 0) __ T (Biological, Ni-63) ~pl=~ in good condition __ are leaking __ are broken 12. 13. 14. 15. 16. f-__ have air bubbles (Only for samples requiring ne beao space) __ Otbc~ Sample pH appropriate for analysis requested Yes [ ] No [ ] NA r ] (lf acidification is necessary go to pH area & document sample ID, initial pH, amount *'HN 3 added and pH nfter addition on table) Were any anomalies identified. in sample receipt? k Yes [ ] No J Description of anomalies (include sample numbers): NA r ] -------· Yes [ ] No Sample Location. Sample Collector Listed on COC? "' *For documentation only. No corrective action needed. Additionalhllonnation:_~=-/~l<~---------------------------------------- ] Client/Courier denied ~empemture check. ] Client/Courier unpack cooler. Sample Check-in 1 completed by Sample Custodian: Signature: ~'-·.::__f~_,·,........=-==-----------D.ate: '\ -'\-\y ~ No action necessary; process as is Project Manngcr 2 <\,.•~..9 Date: By: Person contucted: LS-023 Rev. 17, 05/13 Reviewed 5/2016 Page 1 ofJ TestAmerica Laboratories, Inc. 23 . ·~ Temperaturs on Receipt ---Test America Custody Record Drinking Water? Yes 0 ·No 0 THE LEADER IN ENVIRONMENTAL TESTING TAL ~1£"T\IVYrJ C1lsnt I?JniN-J...UC.t1AI'IAI:: -Olflll..__. r.hafn "' l"'lt.trvlu AJ,~r Tetco _ ·Dean Kitc;hen · l_g;_oz/.201.6 _ _ _ I AddreR;! ·-IlriMMttA NllmbtlrJAmlt.rJ>tfftl/EA>t.NumMr. Lab Mnn/xN 1 l~g~-East 620 South l sot-4n~9106 -. . Page I or Clry • I.Smte_ !-Zla.CoPa ~~-~---l..8b ContBC! I Analysis (Attach list If .~merrcan For!__. ____ Ut j ~AQ03 . u. logans~~mwav___ . m~spsce ~:.;.:n68de::::; . .:.:d:!.~..-...--.--1 ~~t:bJt»J Ci!.rriot/Wsyb/11 NIKrllw [_I · [ Energy Fuels 2016 3rd Quarter _ I 1 I Specisl/nstructionsl eontractiPrJtT:haStt OrdertOuore No. . containers & ! , ~ Conditions of Receipt MatriX Preservatives 'iii I ~ · ~ lj !I ~ N 1 ~ :;;: , 'I ;;J r ~ ::liJ Sample I.D. No. 8lld Description Date Time i 'li! ~ ~ B t; a ~~ , :1 :2 :2 ~ ' F I ~~ ' (ConiMiet$forsachSBmPklmaybscomblnsdononellne) ~ ~ r15 ~ ! ~ ~ ~ ~ ~~ . =&C:-o~~=-1-·-1---1-1---l--+--+--1--------- j Rl DryerBH filter and beaker r -~(22/16 . 113:00 fi ~ l Xl\id.,_/~f4-'f...j...!..f._-i--I--I--I--1--1-------- R1 SYC Scrubber filter and beaker J [ 8/23/16 I ~J.Xl l2li,~1114-.j..:.Y..--l-!.'f.-j.:..)(.-I--+--J----+---4--11---------~ SYC Scrubber filter and beaker I 8/24/16 i 1 12:00 I WL xJ '1:._ f:.-· ;/:::. y., 'f. y. j Rl GrlnlyllaghouseFIIterandBeakl!l' 1 _8/?~(;6 . l 9:00 .I X 7'-X X. X '/... XIX I J __ _ r . . . " --~ .. . ---~+---l--+-4--l--l--1-+--+--i-+-!-+--l--+-l-4-l--l--l--+--+--+-+--l~----- l .. ... . . ~ ---- Poss/b/6 Hazard ld«<li~lion ISsmp/e Disposal (A fll6 may b8 a-d If aamples 8ffJ retaln6d 0 Nori·Ffanrr/ 0 Flammable 0 Skin Irritant 0 Poloon B 0 UnJmown 0 Ratum To Client 0 0/spoeel By Lab 0 Arr:tllve For __ Months 1ongsr than 1 month) Tum Atound Time Required I Q~ RequimnfiiJIS (Specify) 7 Day5 0 14 Day5 0 21 Day5 0 OfJJM:-as..oeLmetilo.d_ r.R, 71me ft. RBceivtld By Ttrntt /).' o0 2. r.me 12. RliCSivadBy '17nii 3. Ref.lnquishiJd By 11m8 I.3.R~By nme .ccmmanta.._ When Complete Email to: Dean or Paul tetco@tetco-ut.com DIBf'RJlW'f'ION:-wRJ'rE-RiitiiiiiiiJ10Ciliiit wit /I Roj)Cit;. CANARY· Stay51Nflflfhe ~; PINK· Rilti Copy J 1 J ] ] . L: "I r l: 1'.': I·. t .. I' APPENDIXD South Yellow Cake Scrubber Figure 1. Facility Schematic Representation Yell ow Cake Dryer Baghouse Figure 2. Facility Schematic Representation Grizzly Baghouse Figure 3. Facility Schematic Representation Process Data South Yellow Cake (Scrubber Flow Rates) Yellow Cake Dryer Baghouse (6 P readings on Field Sheet) Grizzly (tph of material and belt speed) D Facility Energy Fuel Resources t a ~ y Stack Identification: South yell ow Cake Scrubber l+--0~1 13 a: Distance upstream from next disturbance, feet ---- ~: Distance downstream from last disturbance, feet y: Distance of Sample Level to Ground, feet - Estimated Moisture, percent Estimated Temperature, °F . __ Estimated Velocity, fpm ...:-;;;..;·:...;.~:...;...:. __ _ Control Unit Type: Scrubber Number of Ports ~ Figure I. Facility Schematic Representation Process Type: Yell ow Cake Processing Facility= Energy Fuel Resources t a ! y Stack Identification: yellow Cake Baghouse l+---0~1 ~ a: Distance upstream from next disturbance, feet ---- ~: Distance downstream from last disturbance, feet y: Distance of Sample Level to Ground, feet ___ _ 0: Stack Inside Diameter, inches ---- Estimated Moisture, percent Estimated Temperature, °F ----- Estimated Velocity, fpm __ _ --'----- Control Unit Type: Scrubber Number of Ports ~ Figure I. Facility Schematic Representation Process Type: Yell ow Cake Processing ' ,~ .... , _..,..., .- Facility: Energy Fuels t a ! y stack Identification: Grizzly Baghouse l+-0~1 ~ a: Distance upstream from next disturbance, inches 24.5" P: Distance downstream from last disturbance, inches 48" y: Distance of Sample Level to Ground, feet 28' 0 : Stack Inside Diameter, inches 18. 75" Estimated Moisture, percent 1% Estimated Temperature, °F Ambient Estimated Velocity, fpm 775 Number of Ports 2 Process Type: Control Unit Type: ....----------tOre Unloading and Conveying • Baghouse Figure I. Facility Schematic Representation Energy Fuels Resources, Blanding, UT Process Data l / Source: South Yellow Cake Date: &-k_:s /; b Scrubber Flow GPM Time #1 #2 ~p &-~ 0 v -j ~ I . . 5 l ·f <.i-4- ?f: )v ~J .) ( 7 (, :? 2 ~-1 OJ· b ;:) 1 ·) ') 1.1 z1 ·G DJ .; 3 6 l '> 31. ---t I 2 ~ -'-( fD :c.,o --:1 ') ~ (· b z.1-S I 1C· ·. )0 1.2.. .., \ '""1 ;) l. ?l. s \ l 6 D 1.1-3~.l 2\. s \ I .· 3 0 l ·' )u ·Y 2:J--5 IL. ()c) !. \ 3o. 0! 27.2 I \ 2 30 l . i -, A 1l. 2-)C, I /5 .,?0 1· I tf 5o ·Sr "2 i ·"C' (); 3V ~1 . I 3 (J • ----+ 2 -:::) .z l '{: oO 1 -0 ~() .~ z.-:;.-z l L{ _· 30 f:,.~ 29. 5 2l. 2. ( c; : 0 C.--' (o' q 2~. s 27. ?_ ( :, 3c) b-4 2 '1. 5 21, z_ ! ~ ~ c.JU '-:1 . 0 }D·O 21.o I l ~ . )0 1 ·0 ·:S D D z1.--z. Energy Fuels Resources, Blanding, UT Process Data Source: South Yellow Cake Date: B/2..~/l b • Scrubber Flow GPM Time #1 #2 .6.P 7' > 52-D z 1-·u ..-12... ot> J ( Z-: 50 1. I 31.8 2!.~ 15: ov 1· s--~z. c-' -n z 1.-c_ l] : -go -:t·r )z_. () 2-:f·c I~ oo 1 'c;-)Z z. 1· 3 J . •, l l '-{ "_3, 6 1.'-t "32. 2 2l .l IS" DO ).l\ '"\ I 32.?.... ?-' I !(';,() f. ) ~ z__, z_ -z l . \ ,. /'~ 0 0 1--z 3 I . t.(-z ~ -~ t~ ~ 1·] 7\.3 '21' ( ·so , rt-o-v -=\ ') "?..; \ . ~( 'z1. I rt 36 l·--s \ ,....... ~I') 21 .[ ICC 0 0 1·~ )\I v /2. :j -~L .-,. A ... .... fb'" so i. ~ s ,, r) .?? -l . (__ (.. I~ ()0 l ') 3 z. ( 2 -~. (_ l~ 30 l·) 3 z .I z '1-3 ' 20 80 1-·y' 3 2.. 1 2 ).. '2. I rzo 3o 1·c)" ~ 2. D l. ~ ·3 " Energy Fuels Resources, Blanding, UT Process Data Source: Grizz!Y Baghouse Date: '0 / Z..)l?.ol ~ Time Tons (Integrator) tph fpm 8~5( ~ ~lf7o 3a lll\ ( q ·.s9 ~ "1 1Ss 3o t{l-"1-- 1 lo '.c..fo ~{Q 1 3o f' 4.0 U( I~ lt ·. 11--"'7 ~to '{O \l\.Z. l ('.) s ~CP1t..{O) 40 / l ( l. ) rz..·. L -:l-lt"(L{<-{{ y) l tl . .3 l 3: ~~ ~ (:, 1 s ro <oo / l tl I J l~'·Yl. ~,,., 5'3;-)) I\ l~ Z... \tf'.t& ~Co"lS7 ( 3( tlC b tLf'·'-1) G"7bo7 "3_:) Ill' 3 15 '.'Lo ~(., 1 ~t.t{ 'iO \ll ·S \5 '. t.{ ~ ~~l (ol) ~[ lll. ~ I (g :12..-t;, &--r 1 r T 3-r lllaJ l~ :(..{?- ,.._,..-~~lt)) L{o I U. t-( J r ] ] ] J J ~ ,. : ~.:·; .. I' ~ ~,·.:. ·:·:· . ~~ i~ ~ j• r·~. ~ ; ,, ::: . ~ ... k: :r·:i.:· . ' •! I t:-. I i I f,,; APPENDIXE Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature sensors were carried out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 4 Schematic of Method 5/114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-test Dry Gas Meter Calibration Data Forms Type S Pitot Tube Inspection Data Sample Box Temperature Sensor Calibration Balance Calibration E -:---:::: ..... ... :_ .. Temperature Sensor ~ ~Probe ~ .... ·-:--:.'--_ .. ,:::J- I~ Train Qmlal, ~BeRilPated Sf hi Eqoivalenl Condenser ..J TypeS Pilot Tube Temperature Temperature Sensor l Temperature Sensor Nozzle HestThlced Sen.sor~ Gooseneck I ~-------------- lmplngers " ~ ""---""-" / TypeS Pitot Tube ~ Stack Wall Glass Filter Holder Heated Area Manometer Temperature Water Sensors Orifice Empty Silica Gel Figure 4 Schematic of Method 5/114 Sampling Train . .. Vacuum Line I ,- METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES -=''* -~~= 5 ;-g.. = .•Ji r' 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. ENVIRONMENTAL SUPPLY COMPANY 3) Run attested vacuum (from Orifice Calibration Report), for a parfod of «me necessary to achieve a minimum total volume of 5 cubic feel 4) Record data and lnfonnallon In the GREEN caRs, YELLOW cells are calculated. METER SERIAL I:~ CRITICAL ORIFICE SET SERIAL II: G!J EQUIPMENT ID 1: 5J G G z z 2 K' TESTED FACTOR I VACUUM (AVGI (In Hg) 0.1137 jJ 0.8137 13 ·~0 .. 137 13 0.&317 13 0.&317 13 0.6317 13 0.,07 13 0.3307 13 0.3307 13 u .us .u:llo iun 133114 68.04' 7&.4800 82.106 81375 11.030 USING THE CRffiCAL ORIFICES AS CAUBRATlON STANDARDS: 41.630 U.U1 83.3114 8.8.04' 78.4800 12.805 li8.375 ... 03 105.118 s.oos 7.8&1 7.113 &.B&Q 7.418 6.34& 6.670 10.155 1.681 80 77 80 77 ; 10 76 co 72 BO 73 ID 73 80 77 80 74 ·-~ 75 74 74 71 73 72 73 74 75 78 78 • 74 7& 7& !.!.-c...2!... 73 76 76 73 76 76 78 74 74 75 75 78 DOM AVG 7&.26 75.Z5 7&.7& 73.2& 73.Z& 74.00 75.25 74.&0 75.50 Facility FINAL AVG (P.,,J I 25.45 I 25.45 ELAPSED TIME (MINI e §§ 0 0 8.00 1D.i0 8.00 12.60 24.00 15.00 f§ 5 & §§ zo zo § 6 48 2016 Pre-Calibration i&m. &.4757 Ylli ~ Yill Llli! Ulli. !.llli Llill IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED ~ Yn! !.!Mi AVG~ !.illi i.illi Ym AVGa ~ l.lli! .Lm! AVG~ Yn .Mll W! .tni 2m YH 1.lli. un Ul! !!An .2.11! !..IU l :ll.n U!! :2.l!! Tho following oqua1lonc are used to calclEI& the slandard volumiiS of air passed lhrough the DGM. v. (dd), and the critical orifiCe, V., (sld), end the DGM calibration lector. Y. These oquatloos 8111 aulomalically calculaled 11 the spreedsheatabove. AVERAGE DRY GAS METER CALIBRATION FACTOR, y = [ 0.988 I (11 (2) Vm • .,,, = K, • Vm • Pbar + (Mf /13.6) Tm Pbar•E> rcr,_,._,, -K'• .JTctnlb • Net volume of gas sample passed through DGM, corraded to standard conditions K, = 17.&4 'RIIn. Hg (English), 0.3858 'Kimm Hg (Melr1c) T m = Ab!IOiule DGM avg. tomperature ('R • English, 'K ·Metric) ,. Volume or gas sample passed through the cr1tlcal orlflce, corrected to standard conditions T.,. s Aboalute ambient temperalunl ('R • Englith, 'K • Melrlc) K' = Average K' fador tium Critical Orlllca Calibration (ll Vc1e,,,,~, Y= --Vm1..,..., ,. DGM calibration factor Technician: J. Graton AVERAGE AH8 =! 1.639 I 2 AH111" ( 0.75 9 ) AH (Vm(stdJ\ V.,(std) v~ J Tempereture Sen•ora Reference In Out "F "F "F 33 67 202 34 68 203 34 68 203 ~--:_ 1.m !.ill 1..19Q 1&.1! 1.!1! U1I 1.ill !.ill 1..lli. ..,. "---~ .... J' ~ •9• -· fi,,J,,, "'''' l .. { .. rl•tlrl 1 • METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. ENVIRONMENTAL SUPPLY COMPANY 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necassary to achieve a minimum total volume of 5 cubic feel 4) Record data and information in the GREEN cells, YELLOW cells ere calculated. METER SERIAL A!: I ·--· -----I CRITICAL ORIFICE SET SERIAL 1: 14&3S EQUIPMENT ID #: K' TESTED .-----r---t FACTOR I VACUUM (AVGJ (In Hg) G: 0.8137 12 0.8137.; 12 " ,-• .I '0.8137 12 . 688.&02 691.844 ' 897,161 G: 0.5317 12 0.&317 12 0.6317 12 719.006 724.130 7'29.968 G: 0.3307 12 0.3307 12 0.3307 12 702.700 7.08.002 713.083 USING THE CRITICAL ORIACES AS CALIBRATION STANDARDS: 891.844 897.161. 702.610 724.130 729.9&8 73&.196 708.002 713.083 718.238 6.342 6.317 6.349 5.125 5.828 5.238 5.302 5.061 5.175 70 73 . 70 76 70 14 73 78 73 78 73 78 88 89 B8 71 68 74 76 74 78 T8 78 80 71 14 77 70 70 70 70 70 70 ' 70 70 70 70 70 71 66 66 B8 87 87 81 DGM AVG 72 72.26 72.5 74.00 74.00 74.75 68.00 61.50 71.75 FINAL [ 25.66 -1 ELAPSED TIME(MIN) e AVG(P..,) 26.66 §§.00 3.00 . 3.00 1.20 1.20 1.20 §~ 50 50 0 12.50 12.00 12.00 § 44 44 2016 Pre-Calibration Console 9 4.6674 ~ 4.6691 4.3430 ~ 4.432& 4.6342 4.3168 4.3944 IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED l 4.6188 ~ 4.5166 0.1194 4.6168 0.989 AVG= 0.990 .:1,H Mlli !,.Q1§ 5.0031 1.013 Mlli 0.996 AVG= 1.008 Jill 4.5978 ~ 4.4138 1.023 4.4138 1.004 AVG"' 1.014 0.95 !.I§!! 1.ill 1.768 1.651 .1,M! 1:!!!i UH 1.HQ 1,ill. The following equations all! used to calculate lhe standard volumes of a~ passed through lhe DGM, V~ (sld), and lhe crilical orifice, V~ (ski), and the DGM cafibratioo factor, Y. These equations are aulomatically calculated In the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 1.004 I (1) (2) (3) Vmc•"'l = K, * Vm • Pbar + (llH 113.6) Tm Pbar •0 Vcr,,,., = K'• .JTamb = Net volume of gas sample passed through DGM, corrected to standard conditions K1 = 17.64 "RRin. Hg (English), 0.3858 "Kimm Hg (Melricl T m = Absolute DGM avg. lamparatura ("R-English, "I<-Melric) = Volume of gas sample passad through the critical orifica, corrected to standard conditions T..., = Ab&Oiuta ambient temperature ("R -English. "I< -Melricl K' = Average K' factor from Critical Orifice Calibration Vcrc••J Y = -= DGM calibration factor VmC•oll AVERAGE AHa=[ 1.659 I AHa= ( .!!..IU )2 AH (Vm(atd)) V • .(atd) Vm Temperature Sensors Reference In Out "F "F "F 32 33 33 72 73 73 201 202 203 Console 9 Pre-test 2016 :,,·-:·· c,.....:_ :....1 L ... ...... METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES ,. 1M WM*R ee@t J :; 1) Select three critical oriFICes to calibrate the dry gas meter which bracket the expecled operating range. 2) Record barometnc pressure before and after calibration procedure. ENVIRONMENTAL SUPPLY COMPANY 3) Run at tested vacuum (from Orifice Calibration Report), for a period or time necessary to achieve a minimum total volume or 5 cubic reet 4) Record data and information en the GREEN cells, YELLOW cells are calculated DATE;I ••~-·v I METER PART #: Consale 3 METER SERIAL#:~ CRITICAL ORIFICE SET SERIAL II;~ EQUIPMENT 10 #: 2 3 2 3 K' TESTED FACTOR I VACUUM (AVG) (In Hg) . 0:6809 12 0.6808 12 0.~808 12 0.531'7 12 OJI317 12 0.5317 12 473.304 479.30 487.f50 452.700 458.281 464.3980 .-479,30 487.150 493.165 458.281 464.3880 472.119 5.996 7.850 6.015 5.581 6.117 7.721 71J 89 75 90 75 90 75 75 75 78 ~ 81 90 91 90 94 90 94 78 74 81 80 81 82 94 94 96 80 82 84 OOM AVG 91 92 92.50 76.75 80.25 92.00 Facility FINAL f 25.50 I ELAPSED TIME(MIN) 9 AVG (P • .,) 25.50 §E§.oo 2.00 2.00 1.10 1.10 1.10 §.-.. 00 5 00 G G D :1 I I §~ I IIIII :: §§ USING THE CRITICAL ORIACES AS CAUBRATION STANDARDS: Energy Fuels ~ ~ ~ 4.6947 ~ ~ IF Y VARIATION EXCEEDS 2.00'~. ORIFICE SHOULD BE RECALIBRATED l !BQ ~ 6,3816 g,m 4.880 0.990 AVQz 0.991 ~ ~ Ml!! ~ 1:.QQi Mlli 1.003 AVG~ Lm 0.56 AVG: The ldlowing eqmlions life used lo c~cjjate lhe standvd 1/tjumes of 8lf pa~ed !trough llle DGM, Vm (std), end the ailicalllifiCe, Va (std), and lhe OGM cslibrelion faclor, Y, These equalions are auloma~cslly calcllaled in the S!Jeadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 0.996 I (1) (2) l'm1,,, =K, •Fm+ Pbar+(tuf 113.6) Tm VC7·t.uct) = K'• Pbar ... 9 .Jramb = Net volume or gas sample passed through DGM, corrected to standard cond~ions K, = 17.6<4 °Riin. Hg (English), 0.3858 °1</mm Hg (Metric) T m = Absolute DGM avg. temperature ('R -English, °K -Metric) = Volume or gas sample passed through the critical orilice, corrected to standard conditions T..., = Absolute ambient temperature ('R -Englilih, °K -Mebic) K' = Average K' factor hom Critical Orific:a Calibration (3) Vet(,..., Y=~-= DGM calibration factor Vmcndl Technician: K. McNamara AVERAGE t.H0 =Q .571 I t.H,_ = ( 0.76 8 ) 2 t.H (Vm!stdJ\ V .,(std) v.. J Temperature Sensors Reference In Out °F °F °F 33 67 202 34 68 203 34 68 203 1M!! !,ill 1.ru !.ill 1.504 ~ ·""""'··--;..: L. '•' METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after ca~bration procedure. ENVIRONMENTAL SUPPLY COMPANY 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4} Record data and information in the GREEN cells, YELLOW cells are calculated. DATEtl -·-I METER SERIAL *'I ·--· -----I CRITICAL ORIFICE SET SERIAL "' 14535 EQUIPMENT ID #: K' TESTED .-------.---1 FACTOR I VACUUM I I RUN# I (AVG) (In Hg) G: 0.6808 11 I 0.6808 11 l 0.6808 11 I 66.600 74.047 79.734 74.047 79.734 84.989 5.247 5.687 5.255 ~ ~ ~ ~ ~ ~ ~ ~ ~ I ~ ~ 62 i ~ ~ ~ I D :~~ J~ Gtt=j D :~~ 3~ Gtt=j .0 .0 .D .0 .0 .0 FIll II I I I I I I USING THE CRmCAL ORIACES AS CALIBRATION STANDARDS: DGM AVG 62.75 63.50 65 0.00 0.00 0.00 0.00 0.00 0.00 FINAL [2-.;:;J ELAPSED TIME(MIN) 9 AVG(P..,) 24.45 §§.00 2.05 2.06 §§ §§ 4.3577 4.7170 4.3463 Energy Fuels IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 4.3685 4.7325 4.3685 AVG= AVG= AVG= 1.002 ~ 1.006 1.004 t 2,!!!! The following equations are used lo calculate the slandard YOiumes of air passed through the DGM, Vm (sld), and the critical oriftce, v. (std), and the DGM caHbration factor, Y. These equations are automaticaHy calculated lo the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR. y =I 1.004 I (1) (2) (3) I'm.,.,/,= K, •I'm• Pbor+(llH /13.6) Tm f'hur • E> 1~c.:rv,,,1 = K'• .JTnmh = Net volume of gas sample passed through DGM, corrected to standard conditions K, = 17 64 "RRln. Hg (English), 0.3858 "Kimm Hg (Metric) T m = Absolute DGM avg. temperature ("R -English, °K • Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T...., = Absolute ambient temperature ("R -English, "K -Metric) K' = Average K' I actor rrom Critical OrifiCB Calibration l"cJ~-'1411 Y---= DGM calibration factor -r·mur.ll Post test PBrfOIT'Iled byTech Jeff Graton AVERAGEAHg=! 1.789 I 2 AH111 = ( 0.76!! ) AH (Vm(std)\ V"'(std) Vm } Temperature Sensors Reference In Out "F "F "F 32 72 201 33 73 202 33 73 203 !,ill 1.804 1.799 Console 9 Post Test 2016 .xtsx '~ ( ; I. I I 1. TypeS Pitot Tube Inspection Data Date: __ !.:12::.1:..::1 5:!..1:.;;1 5;...__ Pitot Tube ldentification: ____ ___;1:..:8c...G=----- Technician: K. McNamara t p~ Po D,= 0.375 in. Is P" = Pe? Yes Is 1.05 • 0 1 :> P 11 & Pu S 1.50 • D, ? Yes P,.= 0.452 in. Po= 0.452 in. a 1< 10" aJ= al < JO" al~ 2 13J < 5" il1"' ___ o __ 13l < s• Z:>O.I25 in. Z = _......;;0.;.:.0;.;.1.;:.6 __ in. -··· rr-~ ----===:~;...-___ ~:-:·~:.:~ :~ -~.-:r.._~ W :S 0.03125 in. W = ---=0~.0:..:0.;:.5 __ in. W>3 inches W = __ ..;:6;:.;.7..::5 __ in. Z> 3/4 inch Z = __ ..:..:1...:..:75::.__ in. Y;::: 3 inches Y= _-=.3......:.1:..:12~_in. The pitot tube meets the specifications for a calibration factor of0.84? Yes Temperature Sensor Calibration Reference· OmegaCL3512A Probe Continuity Check Yes Heat Check 248 Yes f:l-~ '~ Jemperarure cmpe roture l_emperarure Source Keterence sensor Difference , .. ~~~ (Medium) ("F) ("F) _("F) Probe AJR 65 66 1 AIR 65 64 1 Stack ICE WATER 33 34 1 BOIL WATER 204 204 0 SILICONE OIL b· TypeS Pi tot Tube Inspection Data Date: _ __,;lc:2:...:/lc::.5/:...:1.:;.5 __ Pitot Tube ldentification: ____ __:2:..:7~G=----- Technician: ______ .:.:K::... '-'M:..:c::..N:.:am=a:..:ra,_ ____ _ rs P A= P8 ? ___ _,v,es.:..:.... __ _ Is 1.05•01 s; P,..&P0 S I.SO•D,? ____ Y_es....;.,. __ _ 0.375 in. 0.443 in. 0.443 in. !),= _____ _ Pz= ____ _ Z!,;0.125 in. z = _ __;;o:..:.Oc::.6o=---in. l• ·1" W ~ 0.03125 in. w = _ __;;o.:..:.ooc::.s=---in. -~ ~ -:-Eil-~ · W > 3 inches W = ---'-7 ___ in. Z > 3/4 inch Z= __ ..:.1:.;;:.25~_-in. s u i•. '-' ..... :--<:? ~ ---:11-·------·,, -__ . • _ Y?: 3 inches Y= _ __;;,3~1;.;;/2;..__in. J The pitot tube meets the specifications for a calibration factor of0.84? Yes Ternperarure Sensor Calibrauon Reference· Omega CL3512A Probe Continuity Check Yes Heat Check 248 Yes t~ 1 em perature 1 emperarure 1 em perature Source Reference Sensor Difference (Medium) ("F) ("F) ("F) Probe AJR 68 66. 2 AIR 68 69 I ICE WATER 33 33 0 Stack BOIL WATER 204 204 0 SILICONE OIL TypeS Pilot Tube Inspection Data •·. Date: __ 1"'2/7:...:..:.12::;0:;.;1c:::5 __ Pilot Tube Identification: ____ -=..38~G~-2::_ ___ _ D, Technician: M. McNamara ., ~ : :: _D..:.,~ ____ o...:..3:....7....:s __ in. Is P A= Pa ? ____ Y:....es;:_ __ _ Is 1.05 • D, S P,.& P0 S 1.50 • D, ? ___ ...;Y:.:es=---- 0.458 in. 8:: P11-0.458 in. p, <5" p,= __ ...:._ __ ., Ill <5" P1= ___ 2 __ _ Z S0.125 in. z = _ __::.o.:;.Oc.:.19;;...__in. W S 0.03125 in. W = __ 0:.:·::::02:..4:___in. J. ·-~~ W >3 inches W= 6.5 in. ... Z > 3/4 inch z-2 in. i· ~ -:-ell ! ~=a -~ ... .... ...!.''"¥ ~ ~ ~-:II-----j Y;:: 3 inches Y• 3 112 in - The pilot tube meets the specifications for a calibration factor of 0.84? ~ Temperature Sensor Calibration Reference· Omega CW512A Continuity Check Yes Probe Heat Check 248 Yes r~ 1 emperarure emperatwe ·1 emperature Source Reference Sensor Difference (Medium) ("F) ("F) ("F) Probe AIR 66 65 I AIR 65 65 0 Stack ICE WATER 33 33 0 BOU.WATER 204 204 0 SILICONE OIL '. ··; J. .f ' TETCO Sample Box Temperature Sensor Calibration Date: 12116/15 Calibrator; Alex Moore, Michael McNamara Unit 1D A B c D E F G Thermocouple Location Oven (3} Oven (4) Oven (3) Oven (4) Oven (3) Oven (4) Oven (3) Oven (4) Oven (3) Oven (4) Oven (3) Oven (4) Oven lmpinger Out A lmpinger Out B Impinger Out C Impinger Out D lmpinger Out E lmpingcr Out F Impinger Out G Impinger Out H lmpingcr Out I lmpinger Out J lmpingcr Out K Temperature Source Reference ("F) Reference: Omega CL3512A Temperature Difference \F) .. .•' J I TETCO Sample Box Temperature Sensor Calibration Date: 7/28/16 Calibrator: Alex Moore Reference: Omega CL3512A Box F was destroyed and replaced. This calibration is for the replacement Box F. Thermocouple Temperature TemtJerature Temperature Unit ID Source Reference Sensor Difference Location ("F) ("F) ("F) (Medium) F Oven I Water I 32 31 -1 Water 204 203 -1 i r;r:~Qu,:-s .•: ~-:c~_,,:, lmpinger Out F I Water II 32 I 32 I 0 .· .. _ .. ,_;.::::...-~ Water 204 202 -2 <· 1.·. J TETCO Annual Balance Calibration Check Date 5/12/16 Balance Denver Instruments, Model A-250, SN 8045284 Weights Used Dener Instruments Weight Set, SN 98-115146 Certified Weight Measured Weight grams grams 0.1000 0.0999 0.5000 0.5000 1.0000 1.0001 10.0000 10.0001 50.0000 50.0000 100.0000 99.9999 120.0000 119.9999 150.0000 150.0001 Technician Dean Kitchen Difference _grams 0.0001 0.0000 -0.0001 -0.0001 0.0000 0.0001 0.0001 -0.0001 . . APPENDIXF The testing followed the same procedures as outlined in previous protocols and tests at this facility . ] ] J ) ] Prepared for: Energy Fuels Resources 642SSHwy91 Blanding, Utah 84511 Date of Report: January 4, 2017 FORTH QUARTER RADIONUCLIDE EMISSIONS TEST CONDUCTED AT ENERGY FUELS RESOURCES SOUTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE BLANDING, UTAH November 8-9,2016 by: TETCO 391 East 620 South American Fork, UT 84003 Phone (801) 492-9106 Fax (801) 492-9107 fax J j J ] ] 1 J l J ] ] CERTIFICATION OF REPORT INTEGRITY Technical Emissions Testing Company (TETCO) certifies that this report represents the truth as well as can be derived by the methods employed. Every effort was made to obtain accurate and representative data and to comply with procedures set forth in the Federal Register. " t:-Mike McNamara AI !/ 1~ Reviewer: 'Pf.WJ --~------~~------------- Date:. ______ ,_-_Y_-_1_1 ____ _ Dean Kitchen Reviewer: Date: ' . ( ii } J ) TABLE OF CONTENTS PAGE Introduction Test Purpose ......................................................................................................................... I Test Location and Type ofProcess ...................................................................................... l Test Dates ............................................................................................................................. I Pollutants Tested and Methods Applied ............................................................................. .! Test Participants ................................................................................................................... 2 Deviations from EPA Methods ............................................................................................ 2 Quality Assurance ................................................................................................................ 2 Summary of Results Enrission Results .................................................................................................................. 3 Process Data ......................................................................................................................... 3 Description of Collected Samples ........................................................................................ 3 Discussion of Errors or Irregularities ................................................................................... 3 Percent Isokinetics ............................................................................................................... 4 Source Operation Process Control Devices Operation ..................................................................................... 5 Process Representativeness .................................................................................................. 5 Sampling and Analysis Procedures Sampling Port Location ....................................................................................................... 6 Sampling Point Location ...................................................................................................... 6 Sampling Train Description ................................................................................................. 6 Sampling and Analytical Procedures ................................................................................... 7 Quality Assurance ................................................................................................................ 7 Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence iii LIST OF TABLES PAGE Table I Measured Radionuclide Elllissions ...................................................................................... 3 II Percent Isokinetics ............................................................................................................... 4 III Sampling Point Location ...................................................................................................... 6 IV Complete Results, South Yell ow Cake Scrubber .............................................. Appendix A V Complete Results, Yellow Cake Dryer Baghouse ............................................. Appendix A -] ] LIST OF FIGURES Figure 1 Facility Schematic Representation South Yellow Cake Scrubber ..................... Appendix D 2 Facility Schematic Representation Yellow Cake Dryer Baghouse .................... Appendix D 3 Schematic of Method 5/114 Sampling Train ..................................................... Appendix E ] 1 ] iv l J ] J l 1 INTRODUCTION Test Purpose This test project~as conducted to determine the total radionuclide emissions from the South Yell ow Cake Scrubber and the Yell ow Cake Dryer Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dsct). Test Location and Type of Process Energy Fuels Resources is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Yell ow Cake Dryer Baghouse. The packaging enclosure also discharges into the Yell ow Cake Dryer Baghouse. The South Yellow Cake (SYC) dryer was the only operating dryer at the time of the test. The North Yell ow Cake dryer is currently not operational. Stack schematics are shown as Figures 1 and 2 in Appendix D. Test Dates The first test run on the SYC Scrubber was completed November 8, 2016 and the second run on November 9, 2016. One run was completed on the Yellow Cake Dryer Baghouse November 9, 2016. Pollutants Tested and Methods Applied The tests were a determination of radionuclide emissions in accordance with EPA Method 5/114. The tests for the SYC and the Yellowcake Dryer Baghouse were for the following radionuclide: Th-228, Th-230, Th-232, U-234, U-235, U-238, Pb-210, Ra-226 and Ra-228. Test run fllters and front wash residues were sent to Inter-Mountains Labs located in Sheridan Wyoming for radionuclide analysis. - J ·-] J -] - J ] 1 ] ~ Test Participants Test Facility State Agency TETCO Deviations From EPA Methods None. Quality Assurance Logan Shumway None Jeff Graton Mike McNamara Alex Moore Testing procedures and sample recovery techniques were according to those outlined in the Federal Register and the Quality Assurance Handbook for Air Pollution Measurement Systems. 2 J J J 1 J 1 ) 1 1 SUMMARY OF RESULTS · Emission Results Table I presents the findings of the test in Curies per dry standard cubic foot. Tables IV and V in Appendix A have more detailed information. Table I. Measured Radionuclide Emissions South Yellow Cake Scrubber Yellow Cake Dryer Baghouse Run# pCi/dscf pCilhr pCi/dscf pCilhr 1 26.420 1.127E+06 0.763 8.628E+04 2 12.240 5.152E+05 AVE 19.330 8.212E+05 Test run I on the Yellow Cake Dryer Baghouse was completed with 11 barrels being filled. Process Data The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow, pressure drop readings (..1p) were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (..1p) were recorded and are found on the test run sheets. Production data will be submitted by Energy Fuels Resources. Description of Collected Samples The test filters for the South Yellow Cake Scrubber were heavily covered with a white colored particulate. The front washes were cloudy in appearance. There was no visible particulate matter on the test filter for the Yellow Cake Dryer Baghouse. The front wash was clear in appearance. Discussion of Errors or Irregularities None 3 ] ] ., ] Percent Isokinetic Sampling Each test run was isokinetic within the± 10% of 100% criterion specified in the Federal Register. Isokinetic values for each test run are presented in Table II. Table II. Percent lsokinetic Sam South Yellow Cake Run # Scrubber 1 2 < 102 101 4 Yellow Cake Dryer Baghouse 101 'l':f"7:-~~ •. , • -.:r.;.;. ~-·~-~~~ ,~;~:...._:!~-.. ·~.~ J , J .. ~ -] l ] ] J 1 SOURCE OPERATION Process Control Devices Operation All process control devices were operated normally. Recorded scrubber water flow, pressure and baghouse ~p readings were recorded and are found on the test run sheets or in Appendix D. Process Representativeness The facility was operated normally. Production data was retained by Energy Fuels Resources . s J J J l SAMPLING AND ANALYSIS PROCEDURES Sampling Port Location The inside diameter of the South Yellow Cake Scrubber stack is 12.75 inches. The two, four-inch diameter sample port are located 28.24 diameters (30 feet) downstream from the last disturbance and 6.59 diameters (7 feet) upstream from the next disturbance. Figure 1 in Appendix Dis a schematic of the stack. The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch diameter sample ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 2 in Appendix D. Sampling Point Location Table III shows the distance of each sampling point from the inside wall according to EPA Method 1. Each point is marked and identified with a wrapping of glass tape and numbered. These points are determined by measuring the distance from the inside wall. Distance (inches) from Inside Wall Sample Point SYC Scrubber Dryer Baghouse 1 0.85 0.70 2 3 4 5 6 Sampling Train Description 3.19 9.56 11.90 ;,,_, , .............. --.. -.~· ~'!•~I :_, ______ ~] ! :-. ~-~ ~~ 2.34 4.74 11.26 13.66 15.30 To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-5/114 were followed. All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent interference of the sampled gas and particulate. The stack analyzers used to conduct Methods 1- 5/114 are constructed to meet the specifications outlined in the CFR. The temperature sensors are 6 1 1 J ] ) ] 1 J K-type thermocouples. Heater, vacuwn and pitot line connections have been designed to be interchangeable with all units used by the tester. A 316 stainless steel probe liner was used for the tests. Figure 4 in Appendix Eisa sketch of the Methods 5/114 sampling train. Sample boxes were prepared for testing by following the prescribed procedures outlined in Methods 5/114. Sampling and Analytical Procedures All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 5/114. Quality Assurance All equipment setup, sampling procedures, sample recovery and equipment calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbook for Air Pollution Measurement Systems. 7 J J J 1 1 .. l ] ] ) ] ] J ) APPENDIX A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence 8 J J J J ] l -1 J ] ] APPENDIX A Table IV Complete Results, South Yell ow Cake Scrubber Table V Complete Results, Yellow Cake Dryer Baghouse Nomenclature Sample Equations A TABLE IV SVC Scrubber COMPLETE RESULTS ENERGY FUELS CORPORATION, BLANDING, UTAH SOUTH YELLOWCAKE SCRUBBER EXHAUST 1 Symbol DescriEtion Dimensions Run#l Run#2 Date 11/8/2016 11/9/2016 ., Filter# 6717 6718 Begin Time Test Began 7:45 7:55 End Time Test Ended 15:47 15:57 '1 Pbm Meter Barometric Pressure ln. Hg. Abs 24.75 24.70 I dH <?rificc Pressure Drop In. H20 0.545 0.529 y Meter Calibration Y Factor dimensionless 1.010 1.010 Vm Volume Gas Sampled-Meter Conditions cf 241.715 238.205 Tm Avg Meter Temperature "F 75.3 76.0 VdP Sq Root Velocity Head Root In. H,O 0.2774 0.2738 Wfwc Weight Water Collected Gnuns 140.6 127.5 T, Duration of Test Minutes 480 480 cp Pilot Tube Coefficient Dimensionless 0.84 0.84 ~ Dn Nozzle Diameter Inches 0.3055 0.3055 C02 Volume% Carbon Dioxide Percent 3.20 3.40 02 Volume % Oxygen Percent 16.40 15.80 I N2 &CO Volume% Nitrosen and Carbon Monoxide Percent 80.40 80.80 j Vmstd Volume Gas Sampled (Standard) dscf 199.517 195.957 Vw Volume Water Vapor scf 6.629 6.012 Bws(measured) Fraction H20 in Stack Gas (Measured) Fraction 0.032 0.030 Bws(saruratcd) Fraction H20 in Stack Gas (Saturated) Fraction 0.068 0.072 Bw. Fraction H20 in Stack Gas * Fraction 0.032 0.030 1 xd Fraction of Dry Gas Fraction 0.968 0.970 I ) Md Molecular WI. Dry Gas lbllbmol 29.17 29.18 Ms Molecular WI. Stack Gas lbllbmol 28.81 28.84 1 %1 Percent lsokinetic Percent 101.9 101.4 AVG l T. Avg Stack Temperature "F 95.5 97.0 96.3 A. Stack Cross Sectional Area Sq. Fl. 0.887 0.887 PG Stack Static Pressure ln. H20 -0.030 -0.026 PbP Sample Port Baromelric Pressure In. Hg. Abs 24.68 24.63 Ps Stack Pressure In. Hg. Abs 24.678 24.628 Q. Stack Gas Volumelric Flow Rate (Sid) dscfin 7.1IE+02 7.01E+02 7.06E+02 Qa Stack Gas Volumelric Flow Rate (Actual) cfin 9.37E+02 9.27E+02 9.32E+02 1 v. Velocity of Stack Gas tpm 1.06E+03 1.04E+03 t.OSE+03 Curies Radionuclides per sample pCi 5271.50 2398.83 Curies Radionuclides per blank pCi 0.22 0.22 Net Curies Net Radionuclides per sample pCi 5271.28 2398.61 Crad Concentration of Radionuclides pCi/dscf 26.420 12.240 19.330 ERrad Emission Rate of Radionuclides pCiJhr l.l27E+06 5.152E+05 8.212E+OS * If the measured moisture content is greater than the saturated moisture level (supersaturated), the saturated moisture value will be used in all calculations (40 CFR 60, Method 4, 1 Drvor Baghou11 13 TABLE V COMPLETE RESULTS, PM ., ENERGY FUELS CORPORATION, BLANDING, UTAH YELLOW CAKE DRYER BAGHOUSE S~mbol Descrietion Dimensions Run #1 Date Date 11/9/2016 Filter# 6719 Begin Time Test Began 9:18 J End Time Test Ended 11:20 Pbm Meter Barometric Pressure ln. Hg. Abs 24.70 .6.H Orifice Pressure Drop ln.H10 1.109 y Meter Calibration Y Factor dimensionless 0.999 Vm Volume Gas Sampled-Meter Conditions cf 83.303 Tm Avg Meter Temperature "F 84.9 ..Jt..P Sq Root Velocity Head Root ln. H10 0.4585 Wt_.c Weight Water Collected Grams 12.9 T, Duration ofT est Minutes 120 cp Pitot Tube Coefficient Dimensionless 0.84 J Dn Nozzle Diameter Inches 0.2740 C02 Volwne %Carbon Dioxide Percent 0.00 l 02 Volume % Oxygen Percent 20.90 ' j N2 &CO Volwne% Nitrogen and Carbon Monoxide Percent 79.10 Vmstd Volume Gas Sampled (Standard) dscf 66.790 1 Vw 0.608 Volume Water Vapor scf J Bws Frnction H20 in Stack Gas Fraction 0.009 xd Fraction of Dry Gas Fraction 0.991 Md Molecular Wt. Dry Gas lb/lbmol 28.84 Ms Molecular Wt. Stack Gas lbllbmol 28.74 %1 Percent lsokinetic Percent 100.7 j Ts Avu Stack Temperature "F 100.8 A, Stack Cross Sectional Alu Sq. Ft. 1.396 Po Stack Static Pressure ln. H20 -0.21 PbP Sample Port Barometric Pressure ln. Hg. Abs 24.63 P, Stack Pressure ln. Hg. Abs 24.615 Q. Stack Gas Volumetric Flow Rate (Std) dsclin 1.88E+03 Qa Stack Gas Volwnetric Flow Rate (Actual) clin 2.46E+03 v. Velocity of Stack Gas fpm l.76E+03 "I Curies Radionuclides per sample pCi 5l.l8 Curies Radionuclides per blank pCi 0.22 Net Curies Net Radionuclides per sample pCi 50.96 Crad Concentration of Radionuclides pCildscf 0.763 ERrad Emission Rate of Radionuclidcs pCilhr 8.628E+04 l J ., J ] J '1 J J j Method 5 Nomenclature %1 = percent isokinetic as a percent As = stack cross-sectional area (ft3) ASAP= see.JM> Btu = unit heat value (British thermal unit) Bws = fraction of water in stack gas Cr = concentration of front half particulate matter (gr/dscf, lb/dscf, etc.) Cmetal = concentration of metals (ppm, J.Lg/ft3, etc.). Atomic symbol replaces "metal" C02 = percent carbon dioxide in the stack gas Cp = Pitot tube coefficient Cx (avg) = average concentration of x Cx (corr) = concentration of x corrected to the required percent 02 Deq = equivalent diameter for rectangular stack MI = orifice pressure drop (inches H20) MI@ = orifice pressure (inches H20) Dn = nozzle diameter (inches) Dn des = calculated desired nozzle size (inches) .1P = stack flow pressure differential (inches H20) D5 = diameter of the stack (feet) EA = percent excess air ERr = emission rate of front half particulate (lblhr) ERmmBtu = emission rate per mmBtu or ton of fuel etc. ERx = emission rate of compound. Specific compound replaces x K-fact = multiplier of test point .1P to determine test point MI L = length of rectangular stack (inches) mBtu = thousand Btu Md = molecular weight of stack gas, dry basis (lbnb-mol) Mr = mass of particulate on filter (mg) Mrp = mass of particulate matter on filter and probe (mg) mmBtu = million Btu Mp = mass of particulate matter in probe (mg) M5 = molecular weight of stack gas, wet basis (g/gmol) N2 = percent nitrogen in the stack gas 02 = percent oxygen in the stack gas .JM> = average of the square roots of .1P (may also be referred to as ASAP) Pbm = absolute barometric pressure at the dry gas meter (inches Hg) Pbp = absolute barometric pressure at the sample location (inches Hg) Po = stack static pressure (inches H20) Ps = absolute stack pressure (inches Hg) Pstd = absolute pressure at standard conditions (29.92 inches Hg.) 0 = time length of test (minutes) Qa = stack gas volumetric flow rate (acfm) Qs = stack gas volumetric flow rate (dscfm) Qw = wet stack gas std. volumetric flow (ft3/min, wscfrn) T m = meter temperature (0 F) T5 = stack temperature (°F) Tstd = absolute temperature at standard conditions (528°R) Tt=seeO Vm = sample volume (ft3) at meter conditions ] J J J J ] ] Method 5 Nomenclature Vmstd =volume standard (dsct), sample volume adjusted to 68°F and 29.92 inches Hg. Vs = velocity of stack gas (fpm) V w = volume water vapor (set) at 68°F and 29.92 inches Hg. W = width of rectangular stack (inches) Wtwc = weight of the condensed water collected (grams) X<J = fraction of dry gas Y = meter calibration Y-factor (dimensionless) -.., J -., -1 J -) j J Vw Bws = ----Vmstd+Vw Mrp · 0.01543 Cr = ___,; __ _ Vmstd Method 5 Sample Equations 20.9-desired %02 Cx (carr) = Cx (avg) . 20.9-acrual %02 2·L·W Deq = L W ~~--------~~====~ 0.0269 · (Pbm +0.0735) (Ts +460} ·M5 Dndes = (Tm+460}·Cp·~ Ps·M> %02 -0.5 ·%CO EA = -:--:~---::-:-:--------,-~---::-:--.,....,.,:-:-0.264 · %N2-(%02-0.5 ·%CO) ERr = Cr · Q5 • 0.00857 ERx ERmmBtu = mmBtu/hr 846.72·Dn4 ·MI® ·C2 ·X~ ·Md ·Ps · (Tm +460) K-fact = P Ms · (Ts +460) · (Pbm + #,t) Md = C02 · 0.44 + 02 · 0.32 + N2 · 0.28 Ms = Md·~+18·Bws Vw = Wtwc·0.04715 ~ = 1-Bws J J .I • ! l J } APPENDIXB South Yellow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data Yellow Cake Dryer Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data B . ' ~ I '-" ,-...;, __ 51202_ field Dam She~t Plant: Energy Fuels Date: \IJ'81.1oiL Port ~ Traverse Time Point Clock Min (9) J> I 7.''1) tQ I .::b I ltv .l Lo :;1. go :L laO ~ Do 3 lLf.o 3 lbo Lf J'?P I{ ').;j[) 'i 'llO A I JJ:t.lf_ itto I )...(.p I ~@/ d-. Mt> ;;... 3A-o ;L 7fio j ;)co :3 )'ip 3 LJ_oo !( 4w +-'i'fO Lf?P 15:'1} l.fi,D DGM rn', D"\0 Slt~ /0 ~~ l.f'lo )ITB13. J?..3. til 1~3. 41'1 144. X3l( lt5l5.U._ 1 1<..'1."'13~ ln5.3"e> [Jgs.~a- J'1S_S~ baS. (.~1 I;J.JS, ~8'1 2.15.[5.,(.. 235.25, ~~~.1%~ ;),_S'-/.?,'1~ ,l(,!..j • .115 J+-'1. 11"1 J$3 .es-r J.:'i).5:>i oo3.11& 3Jl._'till 32J..U~ I3~2..J.(,~ ~.-~i .____, .1-P .1-H tin H,OI Vacuum liall:'>l Desired Actual 1mllp:1 19.130 p.'\~ O.'ll{ 2._ b.o~ 0~ 0-.)4 .z. oolt o.S1 o.Sl )... Dofp oSi-a.o ;)_. b ()8} o.s-r los1-3 D.o8\ IOSf.. o.sr 3 ~o81 b,:)'"}·_ DST .3 bc81 (}.')8 Q,_<)f") ;, ~ D. 53> o.$3 4 l) .q]J. o.~l.f o_Sf 1.; o.o1£' D .. ~ o .. .:s-L1 h.olC. tJ 53. D---~ t... o.o7V os~ 6.,)-;L .'j o.of'J-o.S0 o.so L{ O.o1).. O·Sb 0,"\l:l lj D.[).}-~ C),')O D-3V 5 D,o13 (),$'\ oSI ..5 Oot-3 0-51 DSI 5 oor3 OSJ a.SI ;; O.ot-J-b'\0 o • .s1J 5 ?.o71 k:>Sb b.5lJ .::> .'1.Dl-J ln. SO (),0"'0 s '),ato D}L1_ o.'{~ 5 o:o1o (), Ll" o.!f~ ~ •: TErco f1lt~r 6ll)-Smnpk 13oxL Location: South Yellow Cake Dryer Scrubber Operator: A . JJ1 .,..:tft,.... Temperntures, ,., Stack (T,) Probe Oven Filter Effiuent ~1 'J.'l) 2)~ l9S lfl.{ 'to ~S.b 151 1St-~) 1'1 ;tll.)' :.tvg ).'£8 ~(, _5_1 'J..~« .)....":)l:l ).5'0 ~"1 e'fl ~n-;ll.{~ )...~~ s\ '11 .2.50 1~)-)._n I <;.l.. O]j l)IJ 2.Y)_ ).'i)-lsv "'~ ~~., )_I{~ Yt~ 55 "lS' J..ln J.Y'/ '). IJL( Sb 45" :L lf'-1 llJ'1 ')~'( Sf:, 1(, 1'to lh. ).'fl.. X "t(., 2~-D J.-'f) __ J._L/)._ 5C. 9~ 2'38 ;11./3 2'18' (,).... 18 .Z.Sb :Z'I) l'f> ({} 4~ l)..~tt _J._fr ).fj-Ll~ 11 ).'12-JYr l.H ~ 1" ~ ~s-o )..Jo CJ'1 .,, 1'13 21f1 ').l('f ~~ 48 )51-tY"' ).li") 6b t-1~ 2. ~' l--i;"O lh'\1) Sl q1 ;:>,3 15'3 .2..)) S/ '14 'J..tO ~l{ )...)""'1 5lJ 14 J.~'i 2.~~ ).'1~ t{~ f,CP :5£. )... <::,"'tl w 50 t._; I \.. __ _J I L__ll J I Pagl· _l_of_l_ Runll.i._ N1 4 DGM TcmpiTffl) 13 Out In .'58 _sg- Gl lr~ (.1 1?1 .71 17\f rt 78 78 61 &I 8Y 'f<)_ 8Lf 7h 7~ 7.') 78 ~~ 117- 73 7~ ?Y 1( 7Y ~1- 7lf 76 7~ 177 7L{ 11 7J 70 15' 76 7s 78 7~ 71 7C. 7'1 'tt-go 7-;. eo Stack Diameter 12.75" Port Reference __ 0_'_' _ Ports are 7' Upstream from next disturbance Ports are 30' Downstream from last disturbance Assumed Moisture Probe .l.ZL.Cz: Nozzle Calibration 3-5 % Cp~ ~~~ .z/0-.-z:.tX-~ Avg Dn 1~ inches Gas Bag~ J/--07-~ Console 4 -.!--- y -Factor J .oro ~HG J.cStl. in H20 Barometric Pressures Pb,. ). '/, 7$ in Hg Pb0 J 'f. " ~ in Hg Pc ~Q.o3?in H10 Lu k '"""k Pre fQg n·''""" 0,605 D.oOS vac in Hg ..ll -..-l.S:: Pi1o1 Ra1e 0 .0 lnH,O ~ 0 o.LJ' Water Collected ~me Sampled o.D 'i.o O.}..!;"V~~,.,.,..~ JLto . .;;. g '!5:£.. min Total 1:1 1. 7 1.? ./ "G.. 'SrI \:,.ost 2;;t 9 3 "3C /).. R.e v; e.J.£ton'"R1ffi\ ~ .1H@ cclmon ~ 0.).} }'J ~,/. 5(./ 5 .,/ 45, s / ___:1_5.:) / A~~rogt ~ K. 1 Cummenls, ....... ~ t •-.-I I '--J ' "'"--' "-----11 ' '--.-J t __ S/20.:!_ Field Data Sheet Plant: Energy Fuels Date: Jl/1/bJU- Port ~ T 111\'erse Time DGM uP uH ilnH,Ol Vscuum Pain! Clock Min (6) ul'• hnii_.I.)J Desired Actual fitf ~~~' ~' /:JS 0 335.~35 D~l I 0. 'jC( O.Cflf .l I J.o 13'1'"/ I 1l6 0 .of0 lo so tr:CD.S'O ')... , ito I3.S3. S<Jg o.o~ o .c:;-o b.S'"O 2 ,_ Ln [3(..3 . .13'3 0p7o ~,50 o.so h ).... ~ ~7.2 ~ ~.tnl oso lo.~ J_ )... 1110 3U. 41_11 D:)7J ~-,511 C.. SO .2_ 3 IJ.o 13<:11 0~ ~.'ll71 ro.~-o D.~-o :L } llfv llio/ . )t, '3 h.or;L o-->1 O . .f'l 2 ~ J(.o 141 I 1£1-R lo.ors n.~l ln.51 ':3. 'I ~10 l<f J-1 '2'f)._ b.0'70' 0.~ (). f;3 ~ 4 :Jro 1£0 /.Ou.2-P.Dr.3 tJ.Sl lo..s-1 5 'I .l.)O ICI'Io. ?"'t-ID.on-o.s\ 1/J.S"\ 3 A I 11·sJ. l..,O 45o.t..ot-~,D)J. /).,)J I (),.S'I ~ I ).tO 4,0, ~5<=f 0,613 0..5\ lo .. Sl ~ ( ~0 [lf79 10 <0 p,o'(S3 o,~~ o...s~ 3 ,_ ~ Lf~o. 5J t-b,o8_~ 0...:>'1 65"\ '3 J-. 1>d-O [lf\J. lif~ ~.<>8).. O,W 0.16 .3 ).. D~o ISol-~4 b,J~D os\.. D.~~ _:3 ~ ~0 511. X !)'1 b.n80 D ,<)(, ()!c;r, :3 "3 3'f50 51~-13J IO,D'iS'O 0.\(. 0, ")L. :3. 3 4ttJ 53.:2..3go o.o~! O.St osr J q L()() SY'J.._. C.:.l'iS b.<%0 D.St-ost 4 q 4Lfo 5.?~. '025 D.:ffP o,~fo o.::;"b '-( L( Lj(.o ~'5/7) b..)11S o.ss ass-Lf ,r,:6r '180 51:l_tj_l.f Q_----- Total -a.?. 2~lS.~ v,,~S]/4 ~ Av.:roge -J .17 :-;~ v ,5).'\ tl' Comments; '--_J I ~ ----.J Jj l.....-.-o I \....--...-21 ~ . ·~.J I '-~-) '' _,I Jl TETCO Ftlter ~ 71'6 Sample Box__lj_ Location: South Yellow Cake Dryer Scrubber Operator: A /hcnN"r-- Temperatures 11, l'age_l_of_r_ Runll_2_ ('/1 A DGII.I Temp (T nl Stack (T,) Probe Oven Filter Effiuent Out In OB 11 ~~~ 't)... ?55 .:Y3> ').?o 1'1 1255 1'4 1253 "i~ 141 qs-I23Lf 'I~ 2<>3 err :>St, f{j ~51 .,.,. [2_<.,] ~~-2M- 'i~ 'J-'H 48 2:\) Li)O Jj~ lvO 15""' qq 251 44 )liL/ 100 ll/)- j<JO 2,)0 /00 2_1.~ !Oo 25] Joo )..5) 1uo .2.'{1- --- 6 ).32.~ 47.D / l0 .1.')3 .1.5~ l.C,~ ]£'( ')c:;t{ 2\f( :)1.[\ ~$).. :;t53 ~,l. 2Lf7- ;).'lS"" ~Y3 .ll{~ llff ). ~1 )-5]) 24"1 ?-t;')- !lS_4_ ll~f- :~.SJ 25:3 'JSJ 5e> :2$] 'lo/ 1~ '1~ ?-S'"3 Hr J-~1 Sl Jc."Y C,Cf 11.{/ 5L/ ~'iS 53 ';2.9--sr )~") ~ l;.o-Sl l'i1 ~ J.-'is-~ .1'1~ 41 J.'f~ liJ 2lft VJ,. 1~1 Lf.") 1,)0 lff:, :tlf., lf4 2.))... \{1 J.-511 :50 ).~7-51 ;.rJ 5'J ).;)-"') 00 Cp (..j !<'!>Y ~'8 (,'f 7.3 "}2. 7.5' 7<:;" -n> 7€ 81 7~ 7_1 ?(. 17 7:) :r? X' -:r-r 7fo 7g 7C. r1 /" ~-r 75 7-r 7C. 7"\ 1-r 80 ?C. 71 -=n-g.:::> --=rr 80 1-t 50 ?t-~ f'} 7Cf "'R ~ rt-~ Stack Diameter 12.75' Port Reference __ 0_'_' _ Ports are 7' Upstream from next disturbance Ports are 30' Downstream from last disturbance Assumed Moisture 3-5 % Probe ~ Cp_____QM Nozzle Calibration ~ . ')'OJ ~ . "bb~ Avg D. , JCJ..:)'"'S""' inches Gas Bag ....,ll.:91 Console _tj.L.,.... __ Y-Factor J...Q1Q. t.H0 J. Stc,. in H20 Barometric Pressures Pb., l 'i, J'O in Hg Pb0 2t.f.~) inHg Pc -0. 'i>~(:, in H20 Leak Check. Pre Post n'lmin ll.~;:t. Cl.vo-:L '"c in H!!___2.3 N Pitol Rate 0' 0 ~ In H,O ll 0 'j.o O.J....S" o.').:;i" '/)~ Water Collected I)_ 7. 5"" g Time Sampled ':J_go mm ;r-...-.1H@ '?;J (. '1} AV>~ ](,, 0 v' ~o{.tloJ ~Rate A-f,n cclmln ~ @ ... S/t•'4 A .0 Field Data Sheet Plant: Denison Mines Date: '\f.t/ Z.o l \# Travme Time Paint Clock Mln(9) 1 q~ c-9 0 2 10 3 10 4 ~Q 5 Ll..O 6 so 1 10'·1'0 c,o 2 ,o 3 90 4 "" 5 ,,o 6 110 1\'.2.0 tW '-----Jj DGM AP (11~ CloH,Ol "'\'iO·ODcJ .'Z.\ '-4 '{ f.,.ifD .·u .. 'l5l.t,{ •tt. 'lc, \. 0 f.{ ,1.-t 'f(. 8 ·SDcJ • l.( "115.1.('1( . z '3 ..,. t 2 ,(p(, z.. . to 'ftct. S~Q ,1,() 'tel~ :t~to •Zl Sol.ICfo •• 't 56(\. ""'0 ,'Z,o .5 ,,. .S' <.1' w1.0 5'z,'\ 1, lJJ '---"1 ~; 1-TETCO Filter (., 11 SamplcBoxJ!__ AH ~H,Ol Vocuum Desired Actual Clolllll \·~ l.oC( 2.. '·'~ \.1'-1 "'" ... " 2. I·Z1 lo'l.1 z. 6, ···'~ 1.. a. 2.t '· l,.\ 1.- I .oC, l.oC. 1.. \ .. " l•ow ~ t.oct \.o, 2. •• 4)0 1.00 'L ~,.c., l.oc,. """ I • <I<.. l·av '2.. Location: Yellowcake Dryer Baghouse Operator: IV\. ,til !t'l&e-\u-f ~ Temperatures m Stack(TJ Probe Probe Out Filter <Jq 2"10 l ')\ Z.~l 100 'U'f loft. l. ,1.. '"'0 1.{L zt~ 2!3 loO Ul... 'l..{J 1. f'\ ltlll 1.~-( zc.l'l lcr+ lo( 2.(dC) Z.c.&l. Z.ca, to I lC..o l'lltJ l((, lo l Z.1 \ 'Z..f~ z. '" llll t'lo 2.(~ '2.{6 l•t. z. '{-8 tfS l{~ IO 2. "l,.<.( l..(C\ "t{q Jo1.. 2-C.t 'l {~ 1SQ ' Effluent '\,8 &t, "'~ c.) (,'{ S(D 5'1 5( Sl 5( 5.3 5'1 Total ./ e3._3o~ .J s .5o1l ,:,. ~10/' ,1,.01 / A --·-· u -"·"f'b( \· \o'\ \00.10 c-. Time BaghouseAP Time BaghouseAP ,:u, Z..o to'.t"'-l,.( l\ B~~ ~~)1 t.-0 Jb'.Y\ t. ( , •. 1)1. '1.·0 ,o ~s~ 1.·0 ~~~o"'l" t·O n·.o, 1.·0 "---'· '--- DQMTCIIIJI(T.J Out In "11.. 1'1 ,'4 7't 78 8? ?>l ct<, gr 'iz. B< ro Set '0':1-- 8'{ -eq St.f C'f\) 8~ 9v s, Cfo Sf <fO t::..__-'r L -.11 \ Page-_\_of~ I Run II~_ i B I Ao N Stack Diameter _16" __ Port Reference _o.o•_ Ports arc 57" Upstream from next disturbance Ports arc 468" Downstn:am from liSt disturbance Assumed Moisture ' % Probe Z. 1 f--'2.. Cp __!lli. N02%1e Calibration .-z,-4 • z.,"' . t.," . z., &I AvgD. o/.. 7'( inches Gas Bag Ambient Air Console~ Y·Factor • Cf1 Cf -,, t.H0 1 .¥'' mH10 Barometri~ressurcs Pb., t lf. 7° in Hg Pb0 "Zr'l· (,J in Hg Po -r't. l in H20 Lak Checlc: Pre ~ fi'Jmin o · oal VKinH1 ZO·O ...J..Q....s2 Pilot Rate tJ • 0 o. '\) lnH,O 8-i> e.0 Water Collected 12. , g Time Sampled J 10 min to!IC'.f / ~'{. '\ Review /M#iA. _....._:.....0.. __ _ K• @T., K• @T, - . J J ,.,· J .J l 1 J J I -' J Blanding Facility: EnerQI' Fuels Stack Identification: SYC Scrubber ~~~~~------------------------ Date: \I /to /16 Method: 5 IMPINGERS Filter Number: IMPINGERS Filter Number: G~/6 Final (g) Initial (g) Net(gl Final (g) Initial (g) Net(g) Run: ..!., KO I 5(,(,~ SCI B I) jt\. ~ Run: ..!., KO I t_,n ,y 552-.o 'fO I '1 Sample Box: 1-\ 2 liDjnger Number I 3 I ...!.. I s Initial Volume of liquid {H10) in impingcrs, (ml) I 00 I I 00 I MT I SG I ' ' • (, .,, .1-~'12 .-3 ~o,s "11,,)_ "'""(..}, '3 t.,~z.. ~ t..ll.· (, ~1'1.'1.. <S"t.t.C-/ (0 .o n . ~ 'l 'L o Total (g) / LLO , (e / 2 Sample Box: H lmfger Number ..LI 3 I 4 l..i. 6 Initial Volume of liquid (H,O) in impingcrs, (ml) 1ou I 100 I MT I sa ' ' ' ' . (,..:2_\ .J (. '1D. 5"' (..?,) . .) &fJo.o f..o.3. !../ <.:k:J.O (ol),.l ~tf \f.l -)).5' '7.) :>'i.(, Total (g) \)J ;) //"" IMPINGERS Run: Sample Box: Filter Number: 2 lmtger Number I 3 I 4 I s 6 Initial Volume ofliquid (HlO) in impingers, (ml) Ko 100 I 100 I MT I sa Final (g) ____ -+-----+------+-----+------4------- Initial (g) ____ -+------+------+------+------+---- Net(g) =============Z=====d~======-=========== Total (g)======= ------·---· J J .J 'l .J l l I .... j .J J Method 5 Facility: Encrgv Fuels Date: ~11~/-41....£/ ...... J.i.~aal,,.t..-- Stack Identification: Yellow Cake llaghouse Method: ___ ~S---- IMPJNGERS Run: 1 Sample Box: Filter Number: 1 2 imJ!:ger Number I I ..L I s 6 -lnilial Volume of hqu1d (H10) in impingers, (ml) 100 100 I I SG I ' ' . Fin•l<gJ~~ Initial (g) 0: Net(g) '' Ji IMPINGER$ Run: Sample Box: Filter Number: ..L lmfger Number 2 I 3 I 4 I -1-6 Initial Volume of liquid (H20) in impingers, (ml) IOU 100 I I SG I Final (g) ___ -+----+----+-----t----+--- lnilial (g) ___ -+----+----+-----t----+--- Net(g) ============================-====b====== Total (g) ======== IMPINGEBS Run: Sample Box: Filter Number: 2 lmJ!:ger Number I 3 l...i.l s 6 == Initial Volume ortiquid (H20) in impingers, (ml) I 00 I 00 I I SG I Final (g) ___ -+----1----t---~----+--- Initial (g) ----+---;-----r----~-----r----Net(g) ====-===========~====~==-==6===== Total (g)======= J J J J South Yell ow Cake Scrubber Sample Recovery Gas Analysis Data (ORSAT) Yellow Cake Dryer Baghouse Sample Recovery Gas Analysis Data (Ambient) Chain of Custody Lab Analysis APPENDIXC c J J } J J J Plant f~ V\·d <h{ Fv <-l 5 "" Location 6 I o..~ d-v1~ Analytical Method. ____________ _ Date \ \( '5(2.0 l.b Test No. _.:....l -:---::-- Gas Bag No. 14 · o 1- Ambient Temp _1:....0..,..-,..,....__ Operator IA/9f3 Date u{"f{&.ot(. Test No. I. Gas Bag No. 1J ao~ Ambient Temp '10 Operator ~ Date Test No. Gas Bag No. Ambient Temp Operator lr-----T-----~~----~r-----4~-----;-----_,l Ave~ge Net Net Gas Volume 3.2._ 3.2-3 .2 ) '2.- Ave~ge Net Net Gas Volume ).'{ ~·'i >."( ":).'i 3 .. '-f "3.'{ lct.t. l't·t. \{·fJ Ave~ge Net Net Gas Volume C02 t 0 2 was determined using a gas analyzer CO is not measured, as it has the same molecular weight as N2 (__JI L /I liT~: . --------------- Hand Carried l_. __ !; L ---··I C --;; l ----.:1 l-.J L-J Inter-Mountain Labs Sheridan, WYand Gillette, WY 11/09/16 11/09/16 11/08/16 11/09/16 11/09/16 Filter 8:00 9:30 7:45 8:00 9:30 so FT SYC Run 2 6718 Yellow Cake BH 6719 SYC Run 1 6717 Beaker SYC Run 2 6718 Beaker Yellow Cake BH 6719 Beaker ~q Standard turnaround l f RUSH -6 Worttlng Days ,a~ URGENT-< 2 Working Days Rush& Jj --"I L __;1 l L-.JI 1 of 1 FT 1 I X I X I X I X I X I X I X FT 1 lxlxlxlxlxlxlx OT 1 X X X X X X I X OT 1 X X X X X X I X OT 1 X X X X X X I X L /frdl: INTER-MOUliTAIIf LAD;5 CJ Hand Carried [J l . -· L-~-; L---.., L ---·J Inter-Mountain Labs Sheridan, WY and Gillette, WY 11/09/16 8:00 SYC Run 2 6718 ---... 11/09/16 9:30 Yellow Cake BH 6719 11/08/16 7:45 SYC Run 1 6717 Beaker 11/09/16 8:00 SYC Run 2 6718 Beaker 11/09/16 9:30 Yellow Cake BH 6719 Beaker • Standard turnaround £:L RUSH -6 Working Days 1iJ. URGENT-< 2 Working Days Rush & Ument Surt:MfJJH wiJI be l ... t,..P ................. ,_ t ..,a..._ 1-- FT 1 I X I X I X I X I X I X I X FT 1 lxlx1 XIX I XI XIX OT 1 X X X X X X X OT 1 X X X X X X X OT 1 X X -X X X X X .J J .... J J J Use of this system constitutes yqur agreement to the service conditions in the current Fed Ex Service Guide, available on fedex.com. FedEx will not be responsible for any claim in excess of $100 per package, whether the result of loss, damage, delay, non-delivery, misdelivery, or misinformation, unless you declare a higher value, pay an additional charge, document your actual loss and file a timely claim. Limitations found in the current FedEx Service Guide apply. 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IE) Jl513t5081:J»w BILL SENDER TOM PATTON INTER-MOUNTAIN LABS 1673 TERRA AVENUE SHERIDAN, WY 82801 S ip Date: 10NOV16 AcrNgt 6.0 LB MAN Dim: 18 X 16 X 11 iN CAD: 8017201CAFE2915 Ref# lnvoica# PO# Dept## ~ 4732 1453 0634 ~ TUE -15 NOV 4:30P EXPRESS SAVER 82801 SHSHRA wv.us CPR 538C3/CBB1132SB J J J J J ,~ I IYJI: Your Environmental Monitoring Partner Inter-Mountain Labs--------------------------------,J ...... .,., ..... w uu 1673 Terra Avenue, Sheridan, Wyoming 82801 ph: (307) 672-8945 CLIENT: Project: Lab Order: Energy Fuels (White Mesa) Rad Stack Testing 51611262 Date: 1/6/2017 CASE NARRATIVE Report JD: 51611262002 (Replaces 51611262001) Samples SYC Run 1 6717 filter+beaker, SYC Run 12 6718 filter+beaker, and Yellow Cake BH 6719 filter+beaker were received on November 15, 2016. All samples were received and analyzed within the EPA recommended holding times, except those noted below in this case narrative. Samples were analyzed using the methods outlined in the following references: "Standard Methods For The Examination of Water and Wastewater", approved method versions Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW-846, 3rd Edition 40 CFR Parts 136 and 141 40 CFR Part 50, Appendices B, J, L, and 0 Methods indicated in the Methods Update Rule published in the Federal Register Friday, May 18, 2012 ASTM approved and recognized standards The uranium isotopes U234, U235, and U238 ratios are typical for the analysis of natural uranium. The quality checks for mass balance of both uranium and thorium meet expectations. The Regulatory Required Detection Limit (RRDL) was not met for thorium species due to procedureal, matrix and expected air volumes of 6,000,000 mi. The report id S1611262002 replaces 51611262001. This revised report corrects an error found in sample label identification. All Quality Control parameters met the acceptance criteria defined by EPA and Inter-Mountain Laboratories except as indicated in this case narrative. Reviewed by: d.,/~--~---- Wade Nieuwsma, Assistant Laboratory Manager Page 1 of 1 ~ Your Environmental Monitoring Partner Inter-Mountain Labs----------------------------------.:.---,, ...... 0""r••" u•• 1673 Terra Avenue, Sheridan, Wyoming 82801 ph: (307) 672-8945 Sample Analysis Report Company: Energy Fuels (White Mesa) Date Reported 1/6/2017 391 East 620 South ReportiD S1611262002 American Fork, UT 84003 (Replaces 51611262001) ProjectName: Rad Stack Testing Work Order: 51611262 Lab ID: S1611262-001 Collection Date: 11/8/2016 7:45:00 AM ClientSample ID: SYC Run 1 6717 filter+beaker DateReceived: 11/15/2016 9:39:00 AM """' COC: WEB FieldSampler: MM Matrix: Filter Comments Analyses Result Units Qual RL Method Date Analyzed/lnit J Radionuclides -Filter Lead 210 7.1E-06 JJCi/Sample 0.000002 OTW01 12/07/20161021 MB ..., Lead 210 Precision (±) 2.7E-06 JJCi/Sample OTW01 12/07/20161021 MB Radium 226 "1.43E-05 JJCi/Sample 0.0000002 SM 7500RAB 11/30/20161621 MB Radium 226 Precision (:t) 7E-07 JJCi/Sample SM 7500RAB 1 1/30/2016 1621 MB Radium 228 -1.3E0-5 JJCi/Sam[ple 0.0000012 Ga-Tech 12/07/2016 1320 WN Radium 228 Precision (:t) 8.9E-06 JJCi/Sam[ple Ga-Tech 12/07/20161320 WN Thorium 230 1E-07 JJCi/Sample 0.0000002 ACW10 12/09/2016 1258 MB Thorium-230 Precision (:t) 1E-07 JJCi/Sample ACW10 12/09/2016 1258 MB J Thorium 228 -4E-08 JJCi/Sample 0.0000002 ACW10 12/09/2016 1258 MB Thorium-228 Precision (:t) 1E-07 JJCi/Sample ACW10 12/09/2016 1258 MB Thorium 232 OE-07 ~Ci/Sample 0.0000002 ACW10 1 2/09/2016 1258 MB J Thorium-232 Precision (:t) 1E-07 JJCi/Sample ACW10 12/09/2016 1258 MB Uranium 234 2.57E-03 JJCi/Sample 0.0000004 ACW01 12/20/2016 1030 MB Uranium 234 Precision (:t) 3.55E-04 JJCi/Sample ACW01 12/20/2016 1 030 MB Uranium 235 1.10E-04 JJCi/Sample 0.0000004 ACW01 12/20/2016 1030 MB J Uranium 235 Precision (±) 3.17E-05 JJCi/Sample ACW01 12/20/2016 1 030 MB Uranium 238 2.57E-03 JJCi/Sample 0.0000004 ACW01 12/20/2016 1 030 MB Uranium 238 Precision (:t) 4.71E-04 JJCI/Sample ACW01 12/20/2016 1 030 MB Metals-Total Thorium 232 ND )Jg/Sample 45 EPA 200.8 1112212016 1111 MS Uranium 6650 )Jg/Sample EPA 200.8 11122/20161137 MS J J These results apply only to the samples tested. Rl -Reporting Limit Qualifiers: B Analyte detected in the associated MethOd Blank C Calculated Value E Value above quantltation range H Holding times lor preparation or analysis exceeded J Analyte detected below quantltation limits L Analyzed by another laboratory M Value exceeds Monthly Ave or MCL or is less than LCL ND Not Detected at the Reporting Limit 0 Outside the Range ol Dilutions S Spike Recovery outside accepted recovery limits X Matrix Effect Reviewed by: ~4~'-.A""'~~-_::_::_-_-r-_:-_-_:-_-.::_-.,..--- Wade Nieuwsma, Assistant Laboratory Manager Page 1 of 3 J '1 J J J J .... ~ Your Environmental Monitoring Partner .:J..m:.l: Inter-Mountain Labs------------------------------------- '"na-.. ouHYAIH """' 1673 Terra Avenue. Sheridan. Wyoming 82801 ph: (307} 672-8945 Sample Analysis Report Company: Energy Fuels {White M'lsa) Date Reported 1/6/2017 391 East 629 South ReportiD 51611262002 American Fork, UT 84003 (Replaces 51611262001) ProjectName: Rad Stack Testing Work Order: 51611262 Lab 10: 51611262-002 CollectionDate: 1118/2016 9:30:00 AM ClientSample ID: Yellow Cake BH 6719 filter+beaker DateReceived: 11/15/2016 9:39:00 AM COC: WEB FieldSampler: MM Matrix: Filter Comments Analyses Result Units Qual RL Method Date Analyzed/lnit Radionuclides-Filter Lead 210 2.7E-06 pCi/Sample 0.000002 OTW01 12/07/2016 1021 MB Lead 210 Precision (±) 2.7E-06 IJCi/Sample OTW01 12/07/2016 1021 MB Radium 226 1.68E-05 j.JCi/Sample 0.0000002 SM 7500RAB 11/30/20161621 MB Radium 226 Precision (±} 8E-07 j.JCi/Sample SM 7500RAB 11/30/2016 1621 MB Radium 228 -9.2E-06 j.JCVSam[ple 0.0000012 Ga-Tech 12/07/20161624 WN Radium 228 Precision (:} 9.4E-06 j.JCVSam[ple Ga-Tech 12/0712016 1624 WN Thorium 230 1E-07 j.JCi/Sample 0.0000002 ACW10 1 2/09/201 6 1 258 MB Thorium-230 Precision (:) 1E-07 j.JCi/Sample ACW10 12/09/2016 1258 MB Thorium 228 4E-08 IJCi/Sample 0.0000002 ACW10 1 2/09/201 6 1258 MB Thorium-228 Precision (±) 1E-07 j.JCi/Sample ACW10 1 2/09/201 6 1258 MB Thorium 232 4E-08 j.JCi/Sample 0.0000002 ACW10 12/09/20161258 MB Thorium-232 Precision (±) 1E-07 j.JCi/Sample ACW10 12/09/2016 1258 MB Uranium 234 1.24E-5 j.JCi/Sample 0.0000004 ACW01 12/20/2016 1030 MB Uranium 234 Precision (±) 3.66E-4 j.JCi/Sample ACW01 1 2/20/201 6 1 030 MB Uranium 235 O.OE-06 iJCi/Sample 0.0000004 ACW01 12/20/2016 1030 MB Uranium 235 Precision (±) O.OE-06 j.JCi/Sample ACW01 1 2/20/201 6 1 030 MB Uranium 238 1.91E-05 j.JCi/Sample 0.0000004 ACW01 1 2/20/2016 1 030 MB Uranium 238 Precision (±) 4.82E-6 j.JCi/Sample ACW01 12/20/2016 1 030 MB Metals -Total Thorium 232 NO j.Jg/Sample 45 EPA 200.8 11/22/20161114 MS Uranium 80 j.Jg/Sample EPA 200.8 11/22/2016 1114 MS These results apply only to the samples testecl. RL -Reporting Limit Qualifiers: B Analyte detected In lhe associated Method Blank C Calculated Value E Value above quantilatlon range H Holding times for preparation or analysis exceeded J Analyte detected below quantltalion limits L Analyzed by another laboratory M Value exceeds Monthly Ave or MCL or is less lhan LCL NO Not Detected at the Reporting Limit 0 Outside lhe Range-of Dilutions S Spike Recovery outside accepted recovery lim its X Matrix Effect Reviewed by: ..JM~~~;.._,.,...----_-_-_-.,..::::===-- Wade Nieuwsma, Assistant Laboratory Manager Page 2 of 3 J J ] '1 J J J J J J J J l '-' J ~ Your Environmental Monitoring Partner · Inter-Mountain Labs-------------------------------------••m•-.. ou .... ,. u .n 1613 Terra Avenue, Sheridan, Wyoming 82801 ph: (307) 672-8945 Sample Analysis Report Company: Energy Fuels (White Mesa) 391 East 620 South American Fork, UT 84003 ProjectName: Rad Stack Testing LabiD: S1 611262-003 ClientSample ID: SYC Run 2 6718 filter+beaker COC: WEB Comments Analyses Result Radionuclides -Filter Lead 210 9.5E-06 Lead 210 Precision(±) 3.0E-06 Radium 226 1.81 E-05 Radium 226 Precision (±) 8E-07 Radium 228 -4.3E-06 Radium 228 Precision (:1:) 1.1E-5 Thorium 230 lE-07 Thorlum-230 Precision (±) 1E-7 Thorium 228 2E-07 Thorium-228 Precision (±) 1E-07 Thorium 232 3E-08 Thorium-232 Precision (±) 1E-07 Uranium 234 1.18E-03 Uranium 234 Precision (±) 1.73E-04 Uranium 235 6.09E-05 Uranium 235 Precision (±) 1.6E-05 Uranium 238 1.13E-03 Uranium 238 Precision (±) 1.66E-4 Metals-Total Thorium 232 ND Uranium 3450 These results apply only to the samples tested. Qualifiers: B E J M 0 X Analyte detected in the associated Method Blank Value above quantitaUon range Analyte detected below quantitation limits Value exceeds Monthly Ave or MCL or is less than LCL Outside the Range of Dilutions Malrix Effect Date Reported 1/6/2017 ReportiD 51611262002 (Replaces 51611262001) Work Order: 51611262 CollectionDate: 11/8/2016 9:30:00 AM DateReceived: 11/15/2016 9:39:00 AM FieldSampler: MM Matrix: Filter Units Qual RL Method Date Analyzedllnit (JCI/Sample 0.000002 OTW01 12/07/2016 1021 (JCi/Sample OTW01 12/07/2016 1 021 (JCi/Sample 0.0000002 SM 7500RAB 11/30/2016 1621 (JCi/Sample SM 7500RAB 11/30/2016 1621 (JCi/Sam[ple 0.0000012 Ga-Tech 12/07/2016 1928 (JCi/Sam[ple Ga-Tech 12/07/2016 1928 (JCi/Sample 0.0000002 ACW10 12/09/2016 1259 (JCi/Sample ACW10 12/09/2016 1259 j.ICi/Sample 0.0000002 ACW10 12/09/2016 1259 jJCi/Sample ACW10 12/09/2016 1259 (JCi/Sample 0.0000002 ACW10 12/09/2016 1259 j.ICi/Sample ACW10 12/09/20161259 (JCi/Sample 0.0000004 ACW01 12/20/2016 1 030 (JCi/Sample ACW01 1 2/20/2016 1 030 (JCi/Sample 0.0000004 ACW01 12/20/2016 1 030 jJCi/Sample ACW01 12/20/2016 1 030 jJCi/Sample 0.0000004 ACWOl 12/20/2016 1 030 jJCi/Sample ACW01 12/20/20161030 (Jg/Sample 45 EPA 200.8 11122/2016 1118 j.lg/Sample EPA 200.8 11122/2016 1118 Rl -Reporting limit C Calculated Value H Holding times lor preparation or analysis exceeded L Analyzed by another laboratory NO Not Detected at the Reporting Limit S Spike Recovery outside accepted recovery limits Reviewed by: -~.M.....::':"~~~-----__ or-::====::: __ Wade Nieuwsma, Assistant laboratory Manager Page 3 of 3 MB MB MB MB WN WN MB MB MB MB M8 MB MB MB MB MB MB MB MS MS ,j J J J J J J J J '~.. ~ Your Environmental Monitoring Partner ~ Inter-Mountain Labs--------------------------------------••n"-""'""''"'" ''""" 1673 Terra Avenue, Sheridan, Wyoming 82801 ph: (307) 672-8945 ANAL VTICAL QC SUMMARY REPORT CLIENT: Work Order: Energy Fuels (White Mesa) 51611262 Project: Rad Stack Testing Lead 210 in Filters MB-604 (12107/16 12:23) Analyte Lead 210 Lead 210 In Filters LCS-604 (12107/16 10:21) Analyte lead 210 Lead 210 In Filters MS-604 (12107/1610:21) Analyte Lead 210 Lead 210 In Filters MSD-604 (12107/16 10:21) Analyte Lead 210 Radium 228 by GaTTech MB-1695 (12106/16 22:00) Analyte Radium 228 Radium 228 by Gaffech LCS-1695 (12119/16 10:58) Analyte Radium 228 Radium 228 by Gaffech MS-1695 (12119/16 16:27) Analyte Radium228 Radium 228 by Gaffech Qualifiers: MSD-1695 (12121/16 09:56) Analyte Radium 228 B Anal)1e deteclsd In the associalsd Method Blank H Holding times for preparation or :malysis exceeded L Analyzed by another laboratory 0 Outside the Range of Dilutions S Spike Recovery outside accepted recovery limits Sample Type MBLK Date: 1 2/23/201 6 Report ID: 5161 1262001 Units: 1JCi/Sample RunNo: 141552 PrepOate: 11/29116 0:00 BatchiO: R141552 Result Rl Spike Ref Samp %REC % Ree Limits NO 2E-06 Sample Type LCS Units: IJCUSample RunNo: 141552 PrepDate: 11129/16 0:00 BatehiD: R141552 Qual Result Rl Spike Ref Samp %REC % Ree Limits Qual 1E-05 2E-06 1E-05 92.5 eo-147 Sample Type MS Units: ~Ci/Sample RunNo: 141552 PrepDate: 11/29/16 0:00 BatehiD: R141552 Result Rl Spike Ref Samp %REC % Ree limits Qual 1E-05 Sample Type MSD 2E-06 1E-05 NO Units: j.JCi/Sample 101 eo. 143 Run No: 141552 Prep Date: 11129/16 0:00 BatehiD: R1 41552 Result Rl Cone %RPD %REC % RPD limits Qual 1E-05 Sample Type MBLK 2E-06 1E·05 2.29 98.9 20 Units: j.JCi/Sam[ple RunNo: 141993 PrepDate: 11121/16 10:00 BatchiD: 12627 Result Rl Spike Ref Samp %REC % Ree Limits ND 1E-06 Sample Type LCS Units: j.~Ci/Sam[ple RunNo: 141993 PrepDate: 12114116 10:00 BatehiD: 12627 Result Rl Spike Ref Samp %REC % Ree limits 3E-05 Sample Type MS 1E-06 4E-05 87.3 Units: j.JCUSam[ple 63.8-119 RunNo: 141993 PrepDate: 12/14/16 10:00 BatehiD: 12627 Qual Qual Result Rl Spike Ref Samp %REC % Ree limits Qual 1E·06 4E-05 ND 97.0 52.4. 114 4E-05 Sample Type MSD Units: j.JCi/Sam(ple RunNo: 141993 PrepDate: 12/14/16 10:00 Bate hiD: 12627 Result Rl Cone %RPD %REC % RPD Limits Qual 4E-05 1E-06 4E-05 0 94.0 30 E Value above quanlitation range J Analy!e detected below quanlllation lim~s NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits X Malrlx Effect Page 1 of 3 l J l J l u J J ""~-: Your Environmental Monitoring Partner .:1m!; Inter-Mountain Labs----------------------------------_;;_ __ _ tWY« .. •MOUMrAtM LAQ 1673 Terra Avenue, Sheridan, Wyoming 82801 ph: (307) 672-8945 ANALYTICAL QC SUMMARY REPORT CLIENT: Work Order: Energy Fuels (White Mesa) 51611262 Project: Rad Stack Testing Radium 226 Air Filter Analysis MB (11/30/16 00:00) Analyte Radium 226 Radium 226 Air Filter Analysis LCS (11/30/16 00:00) Analyte Radium 226 Radium 226 Air Filter Analysis MS (11/30/16 00:00) Analyte Radium 226 Radium 226 Air Filter Analysis MSD (11/30/1600:00) Analyte Radium 226 Thorium Air Filter Analysis MB-531 (12/09/16 12:56) Analyte Thorium-230 Thorium Air Filter Analysis LCS TH232 (12/13/16 09:17) Analyte Thorium-232 LCS-531 (12109/16 08:38) Analyte Thorium-230 Thorium Air Filter Analysis Qualifiers: LCS0-531 (12/09/16 08:38) Analyte Thorium-230 B Analyte detected In the associalee! Melhod Blank H Holding Umes ror preparation or analysis exceeded L Analyzed by another laboratory 0 Outside the Range or Ollllions S Spike Recovery outside accepted recovery limits Sample Type MBLK Date: 12/23/2016 Report ID: 51611262001 Units: iJCi/Sample RunNo: 141309 PrepOate: 07/11/12 16:00 BatchiD: 12538 Result RL Spike Ref Samp %REC % Rec Limits NO 2E-07 ~ample Type LCS Units: JJCI/Sample RunNo: 141309 PrepDate: 07/11/12 16:00 BatchiD: 12538 Qual Result Rl Spike Ref Samp %REC % Rec Limits Qual 7E-06 Sample Type MS 2E-07 6E-06 119 Units: iJCIISample 70 -130 RunNo: 141309 PrepDate: 07/11/12 16:00 BatchiD: 12536 Result Rl Spike Ref Samp %REC % Rec Limits Qual 8E-06 Sample Type MSD 2E-07 6E-06 NO Units: iJCi/Sample RunNo: 141309 PrepDate: 07/11/1216:00 130 70-130 BatchiD: 12538 Result Rl Cone %RPD %REC % RPD Limits Qual 7E-06 Sample Type MBLK 2E-07 6E-06 5.69 Units: iJCi/Sample 122 30 RunNo: 141792 PrepDate: 11/28/160:00 BatchiD: R141792 Result RL Spike Ref Samp %REC % Rec limits ND 2E-07 Sample Type LCS Units: iJCiiSample RunNo: 141792 PrepDate: 11/28/16 0:00 BatchiD: R141792 Result Rl Spike Ref Samp %REC % Rec Limits 2E-05 2E-07 2E-05 124 68 -146 Run No: 141792 Prep Date: 11/28/16 0:00 BatchiD: R1 41 792 Qual Qual Result RL Spike Ref Samp %REC % Rec Limits Qual 2E-07 1E-05 100 68-146 1E-05 Sample Type LCSD Units: iJCiiSample RunNo: 141792 PrepOate: 11128/16 0:00 BatchiD: R141792 Result RL Cone %RPD %REC % RPD Limits Qual 2E-05 2E-07 1 E-05 22.2 125 30 E Value above quantitation range J Analyte detected below quantitation limits NO Not Detected at the Reporting limit R RPD oLIISide accepted recovery limits X Matrix Effect Page 2 of 3 ..... -~-Your Environmental Monitoring Panner .::1m:~; lnter-Mountam Labs----------------------------------..;;., __ _ ,., Utllii"-MOU"TAlM II.A.S 1673 Terra Avenue, Sheridan, Wyoming 82801 ph: (307)672-8945 ANAL VTICAL QC SUMMARY REPORT CLIENT: Energy Fuels (White Mesa) Date: 12/23/2016 Work Order: 51611262 Report ID: 51611262001 ...... Project: Rad Stack Testing Uranium Isotopic Filters Sample Type MBLK Units: IJCi/Sample MB-26 (12/20/1610:30) RunNo: 141936 PrepDate: 12/15116 0:00 BatchiO: R141936 Analyte Result RL Spike Ref Samp %REC % Rec Limits Qual Uranium 234 NO 4E-07 Uranium 235 NO 4E-07 ., Uranium 238 NO 4E-07 Uranium Isotopic Filters Sample Type LCS Units: IJCI/Sample LCS-26 (12/20/16 10:30) RunNo:141936 PrepOate: 12/15/16 0:00 BatchiO: R141936 Analyte Result RL Spike RefSamp %REC % Rec Limits Qual J Uranium 234 8E-06 4E-07 7E-06 115 50-150 Uranium 235 4E-07 4E-07 4E-07 118 50-150 Uranium 238 SE-06 4E-07 7E-06 117 50-150 Uranium Isotopic Filters Sample Type LCSD Units: IJCl/Sample LCS0-26 (12/20/16 10:30) RunNo:141936 PrepDate: 12/15116 0:00 BatchiD: R141936 Analyte Result RL Cone %RPO %REC % RPD Limits Qual J Uranium 234 8E-06 4E-07 8E-06 2.23 112 20 Uranium 235 SE-07 4E-07 4E-07 13.9 136 20 Uranium 238 91!:-06 4E-07 8E-06 9.75 129 20 J Total (3050) Metals by EPA 200.8-Soil Sample Type MBLK Units: [JQ!Sample MBLK (11/22116 11 :08) RunNo: 141104 Analyte Result RL Spike Ref Samp %REC % Rec Limits Qual J Thorium NO 45 Uranium ND Total (3050) Metals by EPA 200.8-Soil Sample Type LCS Units: IJg/Sample ., LCS (1 1/22/16 10:58) RunNo: 141104 Analyte Result RL Spike Ref Samp %REC % Rec Limits Qual J Thorium 94 45 1E02 94.4 85 -115 Uranjum 91 1 E02 91.1 85-115 Total (3050) Metals by EPA 200.8 -Soil Sample Type MS Units: jlg/Sample S1611262-003AS (1112211611:24) RunNo: 141104 Analyte Result RL Spike RefSamp %REC % Rec Limits Qual Thorium 1010 45 1EOJ NO 91 .7 70-130 Uranium 4280 1 1E03 3450 75.7 70-130 Total (3050) Metals by EPA 200.8-Soil Sample Type MSD Units: [Jg/Sample J S1611262-003AMSO (11/2211611:28) RunNo: 141104 Analyte Result RL Cone %RPO %REC % RPD Limits Qual Thorium 1060 45 1010 5.17 96.6 20 Uranium 4330 1 4280 1.16 80.3 20 .J Qualifiers: B Anal}'le detected in the associated Method Blank E Value above quanUtation range .J H Holding times far preparation or analysis exceeded J Analyte detected below quantltatlon Mmits l Analyzed by anolher laboralar}' ND Not Detected atlhe Reporting Limit 0 Outside lhe Range of Dilutions S Spike Recovery outside accepted recovery lmlts R RPD outside accepted recovery limits X Mab'ix Effect J Page 3 of 3 L a IHTal-MOUHTAIN LldiS a Hand Carried Q L-l L-l-...J L___) Inter-Mountain Labs Sheridan, WY and Gillette, WY Standard turnaround FiHer FT )iii RUSH - 5 Working Days . 0 URGENT -< 2 Working Days Ru~& L.-_J Inter-Mountain Labs. Inc. www llllermountalnlabs com ._.) [ __ of 1 Rev 4 6Web APPENDIXD South Yellow Cake Scrubber Figure 1. Facility Schematic Representation Yellow Cake Dryer Baghouse Figure 2. Facility Schematic Representation .J Process Data South Yellow Cake (Scrubber Flow Rates) Yellow Cake Dryer Baghouse (~ p readings on Field Sheet) J J 1 0 J -11 t___!, L__.,;· L_] _ __..J L-.J Facility: Denison Mines t a ~ y Stack. Identification: South yellow Cake Scrubber l+-0~1 p a: Distance upstream from next disturbance, feet 7' 13: Distance downstream from last disturbance, feet 30' y: Distance of Sample Level to Ground, feet 65' 0: Stack lnside Diameter, inches l 2. 7 5' Estimated Moisture, percenL 4-SI!·o Estimated Temperature, °F I 00-120 Estimated Velocity, fpm 3.000 Control Unit Type: Scnrbbcr NumberofPons 2 ~ Figure 1. Facility Schematic Representation Process Type: L-l Yellow Cake Proc~ssing _J L-JI L___ll [. l lt I L ...Jt F~cility: Denison Mines t <l ! y stack rdentification: Baghouse 1~0-+l I> a:_ Distance upstream from next disturbance, inches 57" fi: Distance downstream ftom last disturbance, inches 454'' y: Distance of Sample Level to Ground, feet · 65' 0: Stack Inside Diameter, inches 16" Estimated Moisture, percent 0-2°/o Estimated Temperature, •r I ..,5 Estimated Velocity, fpm I A-00 Control Uoit Type: Baghouse Number of Ports 1 ~ Figure 2. Facility Schematic Representation Jr __j Process Type: Yello\\ Cakl! Pw~essing J J J l .. -J Energy Fuels Resources, Blanding, UT Process Data Source: South Yellow Cake Date: t \I e{ "LO l b Scrubber Flow GPM Time #1 #2 6P ''.'ft.{ 1.1(,.1 J~,"L-z -a.~ B1r)..o 3.5/ ?. l.. Jfo ,0 :Li.~ '6£~j ~// / ).1. )t~o ?..1.1 4 ',I) 3/5/7, ~ -ss,~ ).7. ~ 1:J)_ 3 .. y /7,J 35.8' 1'),1-' <( {o: Jo 3.~ /7,o 35.~ ))-., lo·. L(t 3.3/7. 0 3s. i J-7, s- 1\ ·. II '3.J/7.0 ·?:,s. 7 )..7.C }) ~ '-1" ).). /7.3 3~.7 )-7.-s--- P ~ rt-'1.1., /1· 3 "3s-. t )_r, Lf )).. : qct :S.f /}.)-3.>. )-)..{,'-( \3',17-Lf,o /7.1 3-l/.1 J-1.!.( ))'.~g' '1,a I 7_1 :>.S:Q )_/, L/ J lf ·.It., 3.~/7, ,_ "'35,s=_ )-7. l( ILf ·-Lft6 ~.~ /7.)-:55S J.:r. lf 15 .' ,., J.~ 17-.1 1.5, lf J_} .)_ t5:L(1-J.<o /7.1 -:>)./ 2.7: 2. ....,- J ] J J ] J J J - J Energy Fuels Resources, Blanding, UT Process Data Source: South Yellow Cake Date: 111~/)..:;>l(... Scrubber Flow GPM Time #1 #2 L\P 6:oo '3J I /..8 'S 51). J-7. y e· . .Jo 3.l(to•1-3{·2-l?,3 9 '.oo ~.?..-{ ~-B '3f."l.-'2_1, ~ 1:")(.. '3.1 /C,~~ 35.7 ).{, 3 /0: ()~ '},I I(,.~ ~5, c ).1. 'f /o: :Ss 3.'1/(_ t 3Y."8' 1.1. "$ ) I :o) '3.~/(6 "7>'5.'/ 27 > , II; 3' 33/t. .. g ) ). 'f )....j,J_ J ') ·.JS J, ~ /'--~ ~s.s ;.?.2 ll.: 31 :3. 3 It -8 )~If .2?. <).. \): 0) l:l.t.,jt.~ "3 ). 53 27. f -Lf,f_j~.f{ 1):3_$ 32.7 .:!::_?-.I }t./: o) ~.(;/t.7 1~.?-J-7. () J tt: ,,. ~.5/,.7-"3S' ., 2,,'1 IS':oy v.5/C? 3>~)_ 210 Jf',J 5 ~.S/&.7 ~).l( 27.o 1s:-: So Lf.S/6.?-?5. ~, 1.?. 0 J J J .- -J J J j APPENDIXE Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature sensors were carried out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 3 Schematic of Method 5/114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-test Dry Gas Meter Calibration Data Forms Type S Pitot Tube Inspection Data Sample Box Temperature Sensor Calibration E -'1 "I 'I 'I ,, L._!! L....J LJI METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES ~ -=-=-· r;,.( wmw""•IWI*fl.ie ~ 1) Select three crilical orifices to calibrate the dry gas meter which bracket !he expected operating range. 2) Record barometric pressure before end arter calibralion procedure. J) Kun altesleO vacuum (!rom Un11ce <..;auDrauon t<epon), tor a penOd o111me necessary to achieve a minimum total volume or 5 cubic feet. 4) Record data and information in the GREEN cells, YEUOW cells are calculated. METER SERIAL#:~ CRITICAL ORIFICE SET SERIAL#:~ EQUIPMENT ID II: K' TESTED ,----,---; FACTOR !VACUUM (AVG) (In Hg) G: 0.5317 11 0.5317 11 0.5317 11 529.501 540.875 540.875 549.822 549.822 657.542 11.374 8.947 7.720 69 69 69 59 91 96 95 47 sa 61 101 73 59 n 79 D:ffi§ D:ffi§ .0 .0 .0 .0 .0 .0 I I II Tl I I I I I I USING THE CRillCAL ORIFICES AS CAUBRA TIOH STANDARDS: (1 FINAL I 25.65 I ELAPSED TlME(MIN) 9 ...-- 65 17.00 80.5 13.00 87.25 11.00 0.00 § 0.00 0.00 0.00 § 0.1111 0.00 AVG(P..,..) 25.65 1.10 § § ~ z.s1n ~ Energy Fuels Bag house IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED ru!m 7.7108 8.5245 AVGe AVG= AVO • 1.025 ~ 1.018 1m ! !!:!!!! The following 9(Jlalions are used to calculate the standaid \l!lkJmeso181T passed lhroog, lhe OGM. V ,.(std), end lhe cntical onfic:e, V" (std) end lhe OGM calibrallon factor, Y Thesa eq~abons are aulomatlcelly calculated m lhe spreadsheet above AVERAGE DRY GAS METER CALIBRATION FACTOR, y = ,-1.023 I (1) (2) Tl"'""' = K, • Tnt• Pbar +(JJi .'13.6) Tm Pbar•e . -K'• r Cl'(so/) -.JTamb = Net volume of gas sample passed through DGM, correcled to standard conditions K, = 17 64 'Rrm Hg (English), 0.3858 "KKnvn Hg (Meine) T" = Absolute 001\A avg temperature ("R -Enghsh, 'I<-Meine) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T .,.,. = Absolute ambient temperabJre ('R -English. "K -Metnc) K' = Average K' factor from Crthcal Orifice Calibration (3) r ·c,;,., r ----, .. ,~~~~=~ = DGM calibration factor Technician: A. Moore AVERAGE AH0 =I 1.486 I 2 t.H0 = ( 0.15 B ) t.H (V..,(std) v • .(stdJ v .. Temperature Sensors Reference In Out °F "F °F 33 67 121 34 66 120 34 66 120 :!.ill .tm 1:!§2 l__..Jj 1.,____3 i L.......Ji ~ L___jr -, L ... METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES ~ ,,. 9 W*ii'I'*MM1yyt;:: • U -· 1) Selec1 three cr~~eal orifices Ia calibrate the dry gas meter which bracket the expec1ed operatong range 2) Rea>rd barometric press~Se before and anot calibration procedure 3) Run attested vacuum (from Orifice Calibrallon Report), for a penod or l1me necessary to ac:tueve a m1n1mum total volume of 5 cub1c reel. 4) Record data and mformat1on "'the GREEN calls, YELLOW cells are calculated OArel ""~' I METER PART 1: Console 4 K' TESTED METER SERIAL I:~ CRITICAL ORIFICE SET SERIAL f:~ ,..-----,---t FACTOR I VACUUM I I RUN .1 (AVGI (In Hal EQUIPMENT ID f: INfllAL DGM AVG G:rnrn G:rnrn • 0 .D ,0 [ I II 1-1 .. 0.3lOT 14 0.3307 14 I 0.3307 14 I 5TU22 514.671 590.196 ~l USIHG THE CRinCAL ORIFICES AS CAUBRATION STA!IDARDS: !!84.671 590.1116 587.000 6.256 6.211 6.104 I T II II 61.5 54 71 49 57 63.5 71 IS 59 69 65 as 94 10 77 S1.7S 71.25 81.50 I FINAL ~ ELAPSED TIME(MW) e AVG(P .. ,) 25.&5 §§ §§ §§~.40 0.40 0.40 ~ ~ 5.1091 Energy Fuels SYC Scrubber IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED ! AVG• AVG= 1Ell !,ill llill 1lli 5.1844 .L.lli. AVG= .L.lli. .!!.!!!!. Thelolowing equations are used lo c;llculate lhe stlnda'd ..,.umes alar passed Hwoogh lhe DGM, v. (std), and lhe cmlcal D<ifice, v. (sld), and the DGM calib<alion lactlf, Y. These equations are auloolatic31y ealeulaled in the ~et above AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = (-1.0!fl (1) (2) ,.,,,,,., = K1•1'm•/'rut•+(!1HII3.6) Tm 1'/wr •0 ,.",.~··'' = A.''• J Ttlllth = Net volufll1> of gas sample passed lhfough DGM. COfrecled to standard condU1ons K, = 17 64 'Riin, Hg (English), 0 3858 'Kimm Hg (Metric) T., = Absolult!!i OGM avg. temperature (8R -English. ex · Metric} = Volume or gas sample passed through the critical orifice. corrected to standard condi11ons T_. = AbsoMe ambiene lemplf'Dwre l~-Engli5h, •K-Metric) K' = Average K' factor from Critical Orifice Callbral.on (3) l'n;>f,,, f= --,.,,l"•l• = DGM calibralion factor T echniclan: A Moore Ice Beth """"""'"" ~Water AVERAGE <!.He =I I 2 <!.He= ( 0.75 Q ) <I.H (Vm(sld)\ V"(sld) Vm J Temperature SensOB Reference In Out "F 33 62 202 "F 33 62 203 "F 33 62 203 _J) Llli U!§ tall L l-JI L_ L L-.1 L-J: L__] _.J j 'j L__j, METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Solecllhrlle crltk:tl orifices 1o cellbralolho dly gas motor which brookellho expt~cled operating range 2) Record barometric prasoure before and ofte< celibrallon procedura. r·=e . v.-M -... ~~ ~~ii! ... ~-«! I, -. - 3) Run attested \IIIQJLI11 (from Orilica C&libnllion Report), lor a ()<Iliad of time nocenary lo ac:hiovo a ninimum lola( 110lumo of 5 cubic fool. 4) Record dala and information In tho GREEN calla, YELLOW cells are calculalaci METER &EIIIAL ''I .. ... I CRrTICAL ORIACE SET aERIAU: 1US& EQUIPMENT ID f: K' TESTED ..-----.---11 FACTOR I VACIAIM I I RUNI (IWOI (11>1101 G G G D.I1J7 UIJ7 0.11S7 0.5>17 1.5311 o.n11 o.no7 0.3307 G..JJ07 11 13 13 ,. 13 13 u 11 13 418.T4G 411.115 UI.D 4>&.377 .U1.111 447.3&2 •n.1'3 UI.IGI 411.113 USING THE CRITICAL ORIFICES AS CAUBRAllON STANDARDS: uuos ut.O 4>1.317 U1.110 U7..J52 uuu UI.HI 41&.113 CT1.1D& 5.126 7.435 I.STT un &.162 U11 1.745 &.2111 '·"' 7G .. Tl II TU TO TO 11 TO TO TO 71 7D 71 TO 75 TO Tl II ,. 71 TO 71 72 7& 15 n " 73 u 74 T4 74 74 T& 75 75 " 71 7& Tl Tl 11 11 75 - •• 71 7Z.OD 7U5 T2.Tl 73.&1 7'-75 71.08 7<1.75 FINAL ~ 13.51 tUG t4.00 AVO(P..,) 25.00 § .. .. !:!.!!! YU! Lml Yll! ~ !.!ill um !J..W Yill 2016 Pra-Callbration IF V VARIATION EXCEEDS 2.10'11, ORIFICE SHOULD BE RECAUBRATED !:!!tl i.1lli uru. AVO• !,!ill !:!!!! !.1m AVG• Y!!! Y!ll Lm! AVO• Y!! Y:!! Y!f 1.!2! .1.ill l.l!l !:!!! llli. .uu !:!!! !,!!§ U!! ! :l!i ~ Y1 1m W! U!! 1!!! !..W W!. ~ l&I 1:!!! The l:>lklwing oqU.1fionl are Uladlocolculalo llo •londard .....,..of ilir paoudilvough llo DGY, v. l•ld), ond 1M crilicolorilioe, V.(•ld).illllt.DGYo:aiibrlllilnlac:lor,Y.n-aquo~~aocniUioonllcaly.-~t.llfll--· AVERAGE DRY' GAS METER CAI.BRATION FACTOR, Y •I 1.0§:) (11 (21 (3J I'm,_= K,• Vm• Pbar+(I1H 113.6) Tnr Phur• 9 Vcr,..,, = K'o .JTamh • Not 110lumo at gos sample passed through OGM. corrected lo otandanj condition& K, • 17.84 "RRIn. Hu tengllsh), D.3115a 'KJmm Htl p.lelr\c) T • ~ AbsolulD DGM •vg. 1Df1'4Jif'81Ure rR • English, •K • Metric) = Volume at !IIIII somplo pauod ltvough lho ctlllcal otlfJCO, correctad lo atanciord <OOdltions T _ = Abs<*oto aml*nlloqJeiOitn t"R • Englsh. "K. Mllldc:J Vt:~j.,,.... r= -r·m, .. w, k' • Ave,.ge I<" .. clor from CriUcal Orttke Catibnllion • OGM calibration factor Technician: _.::J.:.:GB=Ion::::.. ____ _ ........ AtrilloofAM -,.w..., AVERAGE6He~~~ 6He • ( 9.ID )z AH (v .,!atdJ) VaC•tdl v~ Tompenturo Sonaora Raro .. nco In Out "F "F "F 33 62 202 33 62 203 33 52 203 PRE Canoe!. lM CaUboollon 2016.Jdsx L..__jJ L _ _; I L_j I l __ _j I (. _ ___:' I L _ _j , l___.J : L __ J ' L___.JI ~~ L__ji t __ Ji .. 1: \.,. -·----'I L__J, l_ ...JI L _ _]I [_____J I ·-' _ __j 1 ·-' _ _j I METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 11 Select three critical olifices to calibrate tho clry gas meter which bracket tho expeclecl operming range. 2) Record barametric pressure before and after calibration procedure. .... Qi • .._ .a-· ~1i·4/! 3) Run at tested vacuum (fJom Orifice Calibnltlon Report), for s period of time """"SSBIY to achieve a minimum total volume of 5 cubic feel. 4) Record data and information in the GREEN cells, YELLOW cells are CIIICIJated. DATE:~ METER PART II:~ II£TER SERIAL 1:~ CRITICAL ORJACE SET SERIAL#:~ EQUIPMENTID#: G G G 2 3 2 3 2 3 K' TESlED FACTOR I VACUUM (AVGI (In Hg) D.l137 1Z 0.1137 12 0.1137 12 0..5317 12 0.&317 12 0.&317 12 0.3307 12 0.3307 12 0.3307 12 4L2lli M.IIM 62.107 27.302 :M.li81 40.111 lt.llt 7&.644 63.8118 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: ~- 62.107 &11.:10 :M.15111 48.111 47.411 76.644 83.611 11.981 6.4&1 1.111 6.483 7.266 5.660 7.301 7.045 7.048 5.282 73 16 73 17 ~ 10 73 71 73 77 73 11 73 17 73 13 73 63 90 12 ~ 78 12 15 14 u u 7& 77 78 70 71 73 71 78 71 77 78 78 71 73 75 71 71 71 DGM AVG 82 63.& 14.75 72.50 75.7& 71.50 82.26 11.25 81.2& ANAl. AVG(P..,) I 26.70 I 26.70 ELAPSED I I TlME:UIN) §~.06 3.06 3.05 @ 26 .2& E§ DO .50 ~ " M 18.00 16.00 12.00 Y§§ !.!m ~ 6.2117 4.71&11 !.lli!! §.!!!!!! 6.11117 ~ 2016 Pre-Calibration IF Y VARIA TlON EXCEEDS 2.00%, ORIACE SHOULD BE RECAUBRATED 5,4364 ~ 5,4364 AVG• U1!! ~ 6.2166 AVG= !:!!!! !.!!!! ~ AVG= ~ !!,!!! ~ ~ !:!!!!1 ~ .1:.2!!! .1.22! !!,!!! !.HZ P:!!i !:!!I ! ~ 0.51 ~ The lobilg equallans ant used 10 caiWale lhe s1andad 'oiOII.mls o1 ai'passed hough lhe OGM, v,. (~.lnllhe alibi orllce, V,. (stl), and lhe DGM calibr.lllon tactor, V. These aquallans ara auPnati:allycab.(ated In lhe spuadsheat aim&. AVERAGE DRY GAS METER CAUBRAllON FAClOR, Y'" C 0390 (11 (2.1 (31 Vm1,.,11 = K, • Vm• Pbar + (iilf 113.6) Tm Pbar•e ~er,...,, = K.,. ../Tamb 7.045 " Net volume of gas sample passed through OGM, COITIICied to standard conditions K, = 17.64 'Rfn Hg (Engbh), 0 3858 "Kimm Hg (Meine) T,. = AbooUe DGM avg. lomparatu-a ("R ·English."'<· Metric) = Volume of gas sample passed through the critical oriAce, corrected to standard conditions T-= Absoll.Ce umbianl lemp........., ("R -English. "K · Melric) Vcr;Ma~J r~ --Vm(g,, K' ~ Average I<' faclor lrom Critical Orlice Calibration = DGM ca~bralion faciDf Tedlnlcian: --'"''-"'...::Moola="'------ AVERAGEAHe=!-1:665 I AM,. • ( II.Zil )1 AH ~) V.,(std) \ V., Temper.tun1 Sensors Refen~nc:e In Out "f "F "F 33 68 202 33 67 202 33 68 202 .1.IH l.ill .t.m l.I!! ~ .1!!i tm .Lm Yn :....__J, TypeS Pitot Tube Inspection Dam Date: _ _...:.1:21,:..1 5~11:.::5 __ Pitot Tube Identification: ____ ...,!!18:.,::0~---- Technician: K.McNamara t p. Po o,a 0.375 in. Is P•=P8 ? Yes 15 I.OS•D1 ~ P•&P0 ~ 1.50•0,? Yes pAm 0.452 in. PD • 0.452 in. a 1 < 10' a,~ a:< to• a,~ 2 ~·' ~. <s" p,= 0 p,< s" Ill- J ~II, z-~~ Zs0.125in. Z"! 0.016 in. J t c ·-··· '"' ~ ~·~w W s0.03125 in. W= o.oos in. J ~·-··-··--··-·· :~-~ W>3 inches W= 6.75 in. Z> 3/4 inch z-1.75 in. ~±ell J f-£ ~·~~ <i) J + 11-----.;:-1 Y2:.3 inches Y= 3 1/2 in. - The pilOt tube meets the spDCifications for. a calibration factor of0.847 ~ I ::J 1 .., .., J Type S Pitot Tube Inspection Data Dato: __ .::21~5/~16:::..,__ Pitot Tube Identification: ____ .:;27~-:::0-~2:._ __ _ Technician: K. McNamlllll t P, Pa D,m 0.375 pAs 0.450 in. Po= 0.450 in. a1 < 10" a,= 0 a 2< 10° a2~ 0 p, .. __ ..:.o __ ~z= ___ o __ z-~- C Z:S0.125in. Z = -~0~.0:,::16~_in. W :S0.03125 in. W = ---=0~.00'::.!..1 __ in. !-ti~ W>3 inches w .. 6.15 in. Z>3/4 inch Z= 1.5 in. J i =-~·~-·u Q 5._ 1-··--! I ......_! _Y!!:3inchcs Y• 4 112 in. J Tho pitot tube meeiS the specifitalions for a calllmtion factor of0.847 ~ J J J ' .l TETCO Sample ~ox Temperature Sensor Calibration Da111: 12/16/15 Calibrator: Alex Moore, Michael McNamara Thermocouple Location Oven (3) Oven (4) Oven (3) Oven (4) Oven (3) Oven(4) Oven (3) Oven (4) Oven (3) Oven (4) Oven (3) Oven (4) Oven Oven Impinger Out A lmplnger Out B Impinger Out C lmpinger Out D lmpinger Out E lmpinger Out F lmpinger Out G lmpinger Out H Impinger Out I lmpinger Out J Impinger Out K Temperature Source Reference: Omega CL3512A Temperature Difference ("F) ..J -J J -. J J -1 J J l u J APPENDIXF The testing followed the same procedures as outlined in previous protocols and tests at this facility . ATTACHMENT H SURFACE WATER GRAPHS AND FIELD DATA SHEETS 1.00E-05 1.00E-06 1.00E-07 -Q) "i ~.OOE-08 C) .... 0 ...J - 1.00E-09 1.00E-10 1.00E-11 C>.J'b~ ~" ~ •• . - --- - ... ... .... • - '':. --- ~ '::-."OJ rd-cf' Cottonwood Creek Dissolved Radionuclide Concentrations (uCi/ml) -. • .1. .. • • - • ... .6. • • a • -& : - OJOJ~ ~" "rV~ - -- --:. = = ......._... _____ • P;)co ~"Oj rd-10 ~~ ~ ~ "" I • U-Nat. •Th-230 • Ra-226 I ' ~OJ ~ <,j."Oj A ---- .6. • - -,.- ..._b< ~rt' "" .,. ~ <tj.~rt' 1.00E-06 1.00E-07 1.00E-08 -Cl) (U ~.OOE-09 r::n 0 ...1 - 1.00E-10 1.00E-11 1.00E-12 fO<t, ~..._OJ ~"' ...... • ;; -= --• . ~ ~..._OJ cy.~ Cottonwood Creek Suspended Radionuclide Concentrations (uCi/ml) ... -... -• • • ... • T -... -• • ..... .. ..... • • .-= ·------ -------······ ...... ---- -••• • - . PJ<;:) PJ~ PJ<t, PJCO !;:)..._ !;:)b< !;:)co !;:)Oj ..._!'), ..._Q> cl-..._Q) ~..._Q) ~..._OJ ~ ~ ~ ~ ~ ~cv A.'{P ~cv cy.CV ~ ~cv "!\~ ..._<::S ~ ~~ ~'1,; q}.'l; ~~ ~ ..._cv cy. ..._ I • U-Nat. •Th-230 & Ra-226 I - • -... • •• • - -~ - ..._<t, ~ ~ ~ ~cv ~cv ~..._ .... ~ 1.000E+00 1.000E-01 1.000E-02 1.000E-03 1.000E-04 1.000E-05 -Cll ~OOOE-06 C/) m _BoooE-07 - 1.000E-08 1.000E-09 1.000E-10 1.000E-11 1.000E-12 I 1.000E-13 r,::,OJ ~ '\~ - Westwater Creek Dissolved Radionuclide Concentrations (uCi/ml) ~ - ---- "~ ~ \"co "" ~~ ~~~ "~ ~ c6-"~ I • U-Nat. •Th-230 • Ra-226 I "t>< ~ ~ "~\) "I() ~ ~"~ Westwater Creek Suspended Radionuclide Concentrations (uCi/ml) 0.1 ~~~~~~~~~~~~~~~~~~~~~~~~ 0.01 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 0.001 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 0.0001 J'~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~iiii~iiii~ 0.00001 -G) ~.000001 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ ®ooooo1 _. - 1E-09 : i i ' ! 1E-08 1 1E-10 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1E-11 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1 E-12 -1E-13 ;--------------~;-==============:;==============~~~~~~~~~~~~~~~~~~~ ~ ~ ~~!\:) ':-.~'0 ~" "':-.~"' ~" '::..~0;) q}~bi. ,~ ~ ~~ro <t}.~r:;:j ~rv [ • U-Nat • Th 230 /i. Ra-226 I c l. White Mesa Mill-Standard Operating Procedures Book #II: Environmental Protection Manual, Section 2.1 Date: 04/14 Revision: EFR·3 Page5of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one){§Ottonwood Cr~ w ·estwater Canyon Other (describe) ____ _ DA TE:_Cf...L...L...-1 '1.!_.1...1...!.->o./ {,...___ __ pH BUFFER 7.0 __ 7--"---'-.__,_0.._ __ BY: (;f (Sampler's initials) pH BUFFER 4.0 __ '-/"""'-=--, .,0'------ SPECIFIC CONDUCTIVITY _ ____!_l.l!o:<D:.~-D~C~....o2~---~u=M~H~O=s STEAM DEPTH: pH of WATER ----------- CONDeum==h=os~---­ pH Units --------- Temp °C ______ _ COND ~tn=th=os=------- pH units ______ _ Temp °C _______ _ Comments: TEMP ______ _ COND~=rrili==os~----- pH units ______ _ Temp °C _______ _ COND~m==h=os=------- pH units ______ _ Temp °C _______ _ Cottonwood Creek 9/9/2016 Cottonwood Creek 9/20/2016 Cottonwood Creek 9/28/2016 r l White Mesa Mill ·-Standard Operating Procedures Book #11 : Environmental Protection Manual, Section 2.1 Date: 04/14 Revision: EFR-3 PageS ofS Attachment A FIELD WATER ANALYSIS SURF ACE WATER WHITE MESA MILL DATE: ___ q~f~Jo~f~/6~------BY: {-r P (Sampler's initials) pH BUFFER 7.0 __ 7~. """0 __ _ pH BUFFER 4.0 __ 4~-0..L------- SPECIFIC CONDUCTIVITY --"--' O_O_::;.() ____ _,!l=MH=O=s STEAM DEPTH: A/A • pH ofWATER ------------TEMP _______ _ COND =llmh=o=-=s~----COND~=mh==os~---- pH Units ______ _ pH units ______ _ Temp °C ______ _ Temp °C ______ _ COND ~t=mh=os,.__ ___ _ COND~=mh==os~----- pH units ______ _ pH units ______ _ Temp °C -------Temp °C ------- Comments: ... .__ ' :]t•~ Westwater Creek 9/10/2016 Westwater Creek 9/20/2016 Westwater Creek 9/28/2016 White Mesa Mill-Standard Operating Procedures Book #11: Environmental Protection Manual, Section 2.1 ( ... • j Date: 04/14 Revision: EFR-3 Page 5 of 5 Attachment A FIELD WATER ANALYSIS SURF ACE WATER WHITE MESA MILL LOCATION (Circle on :Cottonwood Creek Westwater Can on Other (describe) ____ _ DATE: I z.l Cr II ~ BY:_-loo&t::.....JP!....--____ _ (Sampler's initials) pH BUFFER 7.0 _-..e7c....;.·..::O~--pH BUFFER 4.0 -~...:...:·J,.D.t__ __ _ SPECIFIC CONDUCTIVITY _.-~,..;I O~O...lo..O.{....._ ____ -l:!u=MH~O~s STEAM DEPTH: pH ofWATER -----------TEMP _______ _ COND 1=!-!J.lm=ho~s:...._ ___ _ COND~rnh~~os~---- pH Units ______ _ pH units ------- Temp °C -------Temp °C ------- COND ~-=mh=o=-s ____ _ COND ~-~mh~o~s ____ _ pH units ______ _ pH units------- Temp °C ______ _ Temp °C ______ _ Comments: ( White Mesa Mill -Standard Operating Procedures Book #11: Environmental Protection Manual, Section 2.1 Date: 04/14 Revision: EFR-3 Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one):Cottonwood Creek (Westwater ~{)ther (describe) ____ _ BY:_~6:~· p'----------- (Sampler's initials) pH BUFFER 7.0 __ 7--'-'-.~0£..._ __ pH BUFFER 4.0 _ _:4 ...:.. • .:::..() ___ _ SPECIFIC CONDUCTIVITY _..._I O"""O&....u...O~--------t::tl=MH=O=s STEAM DEPTH: pH ofWATER -----------TEMP ___________ _ COND ~:Um=h~o~s ____ __ COND~t.~rrili~os~----- pH Units -------pH units ______ _ Temp °C ______ _ Temp °C ______ _ COND ~·=mh=os=-------COND ~.,.,rrili=os~---- pH units ______ _ pH units ------- Temp°C _______ __ Temp °C ______ _ Comments: ~ ~ ~ \0 u -1-< 0 ~ ~ ..... ro 0'1 ~ ..._ ..... N rJ) -~ ~ EN:RGY Trust our People. Trust our Data. www.e nergylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 88&.886.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 09:00 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-053 Client Sample ID: WestWater Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units ND wt% 0.1 mg/kg-dry 0.05 pCi/g-dry 0.09 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.04 pCilg-dry 0.05 pCilg-dry 0.01 pCilg-dry 0.1 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D u u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:14/ smm 0.03 SW6020 09/02116 22:171 sf E909.0 10/02/16 19:46 I eli-cs E909.0 10/02116 19:46 I eli-cs E909.0 10102116 19:46/ eli-cs E903.0 09119116 14:19/ dmf E903.0 09119116 14:191 dmf E903.0 09119116 14:191 dmf E908.0 09116116 09:36 I eng E908.0 09116116 09:361 eng E908.0 09/16116 09:36/ eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 57 of70 EI\ERGY Trust our People. Trust our Data. www.eneryylab.com Billings, MT 800.735.4488 • Casper, WY 888.235.0515 Collage station, TX 888.890.2218 • Gillette, WY 888.888.7175 • Helena, MT 877.472.0711 February 03, 2017 Energy Fuels Resources (USA) Inc 225 Union Blvd Ste 600 Lakewood, CO 80228-1826 Work Order: C 16080582 Project Name: Annual Soils 2016 ANALYTICAL SUMMARY REPORT Energy Laboratories, Inc. Casper WY received the following 56 samples for Energy Fuels Resources (USA) Inc on 8/12/2016 for analysis. LabiD Client Sample ID Collect Date Receive Date Matrix Test c 16080582-001 N01 08/09/16 8:26 08/12116 Soil Metals by ICP/ICPMS, Total Percent Moisture Digestion For RadioChemistry Lead 210 Radium 226 Thorium, Isotopic c 16080582-002 N02 08/09/16 8:52 08/12/16 Soil Same As Above c 16080582-003 N03 08/09/16 8:54 08/12116 Soil Same As Above c 16080582-004 N04 08/09/16 9:01 08/12/16 Soil Same As Above c 16080582-005 NOS 08/09/16 9:02 08/12/16 Soil Same As Above c 16080582-006 E01 08/09/16 9:08 08/12/16 Soil Same As Above c 16080582-007 E02 08/09/16 9:12 08/12/16 Soil Same As Above c 16080582-008 E03 08/09/16 9:16 08/12/16 Soil Same As Above c 16080582-009 E04 08/09/16 9:18 08/12/16 Soil Same As Above c 16080582-010 E05 08/09/16 9:23 08/12/16 Soil Same As Above c 16080582-011 E06 08/09/16 9:27 08/12/16 Soil Same As Above C16080582-012 EO? 08/09/16 9:30 08/12/16 Soil Same As Above C16080582-013 E08 08/09/16 9:51 08/12/16 Soil Same As Above c 16080582-014 E09 08/09/16 9:56 08/12/16 Soil Same As Above c 16080582-015 E10 08/09/16 9:59 08/12/16 Soil Same As Above C16080582-016 E11 08/09/16 10:02 08/12/16 Soil Same As Above c 16080582-017 E12 08/09/16 10:08 08/12/16 Soil Same As Above c 16080582-018 E13 08/09/16 1 0:20 08/12/16 Soil Same As Above c 16080582-019 E14 08/09/16 10:26 08/12/16 Soil Same As Above c 16080582-020 E15 08/09/16 10:28 08/12/16 Soil Same As Above c 16080582-021 E16 08/09/16 10:33 08/12/16 Soil Same As Above c 16080582-022 E17 08/09/16 10:39 08/12/16 Soil Same As Above c 16080582-023 E18 08/09/16 1 0:44 08/12/16 Soil Same As Above c 16080582-024 S01 08/09/1610:51 08/12/16 Soil Same As Above Page 1 of 70 EI\ERGY Trust our People. Trust our Data. Billings, MT 800.735.4489 • Casper, WY 888.235.0515 www.energylab.com College Station, TX 888.890.2218 • Gillette, WY 888.886.7175 • Helena, MT 877.472.0711 ANALYTICAL SUMMARY REPORT c 16080582-025 S02 08/09/16 8:30 08/12/16 Soil Same As Above c 16080582-026 S03 08/09/1612:47 08/12/16 Soil Same As Above c 16080582-027 W01 08/09/16 8:31 08/12/16 Soil Same As Above c 16080582-028 W02 08/09/16 8:38 08/12/16 Soil Same As Above c 16080582-029 W03 08/09/16 8:43 08/12/16 Soil Same As Above c 16080582-030 W04 08/09/16 8:46 08/12/16 Soil Same As Above c 16080582-031 W05 08/09/1613:51 08/12/16 Soil Same As Above c 16080582-032 W06 08/09/16 13:4 7 08/12116 Soil Same As Above c 16080582-033 W07 08/09/16 12:44 08/12/16 Soil Same As Above c 16080582-034 W08 08/09/16 13:40 08/12/16 Soil Same As Above c 16080582-035 W09 08/09/1613:36 08/12/16 Soil Same As Above c 16080582-036 W10 08/09/1613:33 08/12/16 Soil Same As Above c 16080582-037 W11 08/09/1613:13 08/12/16 Soil Same As Above c 16080582-038 W12 08/09/1613:16 08/12/16 Soil Same As Above c 16080582-039 W13 08/09/16 13:22 08/12/16 Soil Same As Above c 16080582-040 W14 08/09/16 13:26 08/12/16 Soil Same As Above c 16080582-041 W15 08/09/16 12:57 08/12/16 Soil Same As Above c 16080582-042 W16 08/09/1612:33 08/12/16 Soil Same As Above c 16080582-043 W17 08/09/1612:37 08/12/16 Soil Same As Above c 16080582-044 W18 08/09/16 12:42 08/12/16 Soil Same As Above c 16080582-045 BHV-1 08/09/16 9:04 08/12/16 Soil Same As Above c 16080582-046 BHV-2 08/09/16 9:42 08/12/16 Soil Same As Above c 16080582-04 7 BHV-3 08/09/16 9:23 08/12/16 Soil Same As Above c 16080582-048 BHV-4 08/09/16 10:12 08/12/16 Soil Same As Above c 16080582-049 BHV-5 08/09/16 9:54 08/12/16 Soil Same As Above c 16080582-050 BHV-6 08/09/16 10:05 08/12/16 Soil Same As Above c 16080582-051 BHV-7 08/09/16 9:21 08/12116 Soil Same As Above c 16080582-052 BHV-8 08/09/16 8:58 08/12/16 Soil Same As Above c 16080582-053 WestWater 08/09/16 9:00 08/12/16 Soil Same As Above c 16080582-054 E65 08/09/16 10:02 08/12/16 Soil Same As Above c 16080582-055 W70 08/09/1613:51 08/12/16 Soil Same As Above c 16080582-056 S75 08/09/16 8:30 08/12/16 Soil Same As Above The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Page 2 of 70 EN:RGY Report Approved By: Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4488 • Casper, WY 888.235.0515 College Station, TX 888.690.2211 • Gillette, WY 888.888.7175 • Helena, MT 177.472.0711 ANALYTICAL SUMMARY REPORT Digitally signed by Corinne Wagner Date: 2017.02.03 08:58:22 -07:00 Page 3 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.(om Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Colleee Station, TX 888.890.2218 • Gillette, WY 866.688.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 08:26 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: C16080582-001 Client Sample ID: N01 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.3 mglkg-dry 0.6 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.05 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:281 smm 0.03 SW6020 08131116 21 :341 sf E909.0 09128116 11 :44 I eli-cs E909.0 09/28/16 11 :44 I eli-cs E909.0 09128116 11 :44 I eli-cs E903.0 09114116 07:441 dmf E903.0 09114116 07:441 dmf E903.0 09114116 07 :441 dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 5 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.680.2218 • Gillette, WY 866.886.7175 • Helena, MT 871.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 08:52 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-002 Client Sample ID: N02 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units ND wt% 0.3 mg/kg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.6 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.5 pCilg-dry 0.09 pCilg-dry 0.1 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:281 smm 0.03 SW6020 08131116 21:36/ sf E909.0 09128116 13:27 I eli-cs E909.0 09/28116 13:27 I eii-cs E909.0 09128116 13:27 I eli-cs E903.0 09114/16 07:44 I dmf E903.0 09114/16 07:44 I dmf E903.0 09114/16 07:441 dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114/16 09:57 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -Rl increased due to sample matrix. Page 6 of70 EN:RGY Trust our People. Trust our Data. www.eneryylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 888.888.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 08:54 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-003 Client Sample ID: N03 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units ND wt% 0.3 mg/kg-dry 0.6 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.4 pCilg-dry 0.07 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15116 10:281 smm 0.03 SW6020 08131116 21:391 sf E909.0 09128116 06:35 I eli-cs E909.0 09128116 06:351 eli-cs E909.0 09128116 06:351 eli-cs E903.0 09114116 07:44 I dmf E903.0 09114116 07:44 I dmf E903.0 09114116 07:44 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 7 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 09:01 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-004 Client Sample ID: N04 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.6 wt% 0.2 mglkg-dry 0.6 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.7 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.4 pCilg-dry 0.07 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15/16 10:29 I smm 0.03 SW6020 08131116 21 :411 sf E909.0 09128116 15:10 I eli-cs E909.0 09128116 15:10 I eli-cs E909.0 09128116 15:10 I eli-cs E903.0 09114116 07:44 I dmf E903.0 09114116 07:44 I dmf E903.0 09114116 07:44 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 8 of70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4488 • Casper, WY 888.235.0515 College station, TX888.890.2218 • Gillette, WY 866.888.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:02 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-005 Client Sample ID: NOS Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 1.6 wt% 0.5 mglkg-dry 0.5 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.9 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.4 pCilg-dry 0.07 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:291 smm 0.03 SW6020 08131116 21:441 sf E909.0 09128116 16:531 eli-cs E909.0 09128116 16:531 eli-cs E909.0 09128116 16:53 I eli-cs E903.0 09114116 07:44 I dmf E903.0 09114116 07:441 dmf E903.0 09114116 07:441 dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 9 of70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 888.886.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 09:08 DateReceived: 08/12116 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-006 Client Sample ID: E01 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.0 wt% 0.9 mglkg-dry 0.5 pCi/g-dry 0.2 pCi/g-dry 0.2 pCi/g-dry 1.4 pCilg-dry 0.3 pCilg-dry 0.04 pCilg-dry 0.3 pCi/g-dry 0.06 pCi/g-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15116 10:291 smm 0.03 SW6020 08/31116 21:46/ sf E909.0 09/28116 18:361 eli-cs E909.0 09/28116 18:361 eli-cs E909.0 09128116 18:36 I eli-cs E903.0 09114/16 07:441 dmf E903.0 09/14/16 07:441 dmf E903.0 09114116 07:441 dmf E908.0 09/14/16 09:57 I eng E908.0 09/14/16 09:57 I eng E908.0 09114/16 09:57 I eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 10 of70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09116 09:12 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-007 Client Sample ID: E02 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 1.4 wt% 0.7 mgfkg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 1.7 pCi/g-dry 0.3 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.04 pCi/g-dry 0.1 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:29 I smm 0.03 SW6020 08131116 21:58/ sf E909.0 09128116 20:19 I eli-cs E909.0 09128116 20:19 I eli-cs E909.0 09/28116 20:19 I eli-cs E903.0 09/14116 07:44 I dmf E903.0 09/14116 07:44 I dmf E903.0 09/14116 07:44 I dmf E908.0 09114116 09:57 I eng E908.0 09/14/16 09:57 I eng E908.0 09/14/16 09:57 I eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 11 of 70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Colleee Station, TX 888.890.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LA BORA TORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:16 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-008 Client Sample ID: E03 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.8 wt% 0.9 mglkg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.2 pCi/g-dry 1.6 pCilg-dry 0.3 pCilg-dry 0.04 pCilg-dry 0.3 pCilg-dry 0.06 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:30 I smm 0.03 SW6020 08131116 22:01 I sf E909.0 09128116 22:021 eli-cs E909.0 09128116 22:02 I eli-cs E909.0 09128/16 22:02 I eli-cs E903.0 09114116 07:44 I dmf E903.0 09114116 07:44 I dmf E903.0 09114116 07:441 dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 12 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.890.2218 • Gillette. WY 866.886.7175 • Helena, MT 877.412.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:18 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 LabiD: c 16080582-009 Client Sample ID: E04 Analyses PHYSICAL CHARACTERISTICS Moisture METALS • TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.9 wt% 1.1 mglkg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 1.3 pCilg-dry 0.3 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:30 I smm O.D3 SW6020 08131116 22:03/ sf E909.0 09128116 23:46 I eli-cs E909.0 09128116 23:46 I eli-cs E909.0 09128116 23:461 eli-cs E903.0 09114116 07:44 I dmf E903.0 09114116 07:441 dmf E903.0 09114116 07:441 dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 13 of 70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 88&.88&.7175 • Helena, MT 877.472.0711 LA BORA TORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 09:23 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-01 0 Client Sample ID: E05 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADION UC Ll DES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.3 wt% 3.2 mglkg-dry 0.3 pCilg-dry 0.1 pCilg-dry 0.2 pCilg-dry 4.0 pCilg-dry 0.8 pCilg-dry 0.04 pCilg-dry 0.3 pCilg-dry 0.05 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:30 I smm 0.03 SW6020 08131116 22:061 sf E909.0 09129116 01 :29 I eli-cs E909.0 09129116 01 :29 I eli-cs E909.0 09129116 01:29 I eli-cs E903.0 09114116 07:44 I dmf E903.0 09114116 07:441 dmf E903.0 09114116 07:44 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 14 of70 EN:RGY Trust our People. Trust our Data. www.eneryylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 188.890.2218 • Gillette. WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:27 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: C16080582-011 Client Sample ID: E06 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units NO wt% 4.3 mglkg-dry 0.4 pCI/g-dry 0.2 pCi/g-dry 0.2 pCilg-dry 4.0 pCilg-dry 0.8 pCIIg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:411 smm 0.03 SW6020 08131116 22:08/ sf E909.0 09129116 03:12 I eli-cs E909.0 09129116 03:12 I eli-cs E909.0 09/29/16 03:121 eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant leveL ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 15 of70 EN:RGY Trust our People. Trust our Data. www.e ne rgylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.688.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:30 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab 10: C16080582-012 Client Sample 10: E07 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.5 mglkg-dry 0.06 pCilg-dry 0.1 pCilg-dry 0.2 pCilg-dry 1.2 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.08 pCilg-dry 0.02 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:411 smm 0.03 SW6020 08131116 22:111 sf E909.0 09129116 04:55 I eli-cs E909.0 09/29116 04:551 eli-cs E909.0 09129116 04:55 I eli-cs E903.0 09114/16 09:40 I dmf E903.0 09114/16 09:40 I dmf E903.0 09114/16 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 16 of 70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 886.886.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:51 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: C16080582-013 Client Sample ID: E08 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 0.3 wt% 2.4 mglkg-dry 0.5 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 3.5 pCilg-dry 0.7 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:42 I smm 0.03 SW6020 08131116 22:13 I sf E909.0 09129116 06:38 I eli-cs E909.0 09129116 06:38 I eli-cs E909.0 09129116 06:38 I eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 17 of 70 Er\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Collage station, TX 888.890.2218 • Gillette, WY 866.886.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:56 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: C16080582-014 Client Sample ID: E09 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 0.4 wt% 2.0 mglkg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 2.5 pCilg-dry 0.5 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:421 smm 0.03 SW6020 08131116 22:161 sf E909.0 09129116 08:21 I eli-cs E909.0 09129116 08:21 I eli-cs E909.0 09129116 08:21 I eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 18 of 70 Er\ERGY Trust our People. Trust our Data. www.eneryylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.886.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:59 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-015 Client Sample ID: E10 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 0.7 wt% 1.6 mglkg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 2.0 pCilg-dry 0.4 pCilg-dry 0.04 pCilg-dry 0.3 pCilg-dry 0.06 pCilg-dry 0.1 pCilg-dry MDC - Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:421 smm 0.03 SW6020 08131116 22:181 sf E909.0 09129116 10:041 eli-cs E909.0 09129116 10:041 eli-cs E909.0 09129116 10:04 I eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -Rl increased due to sample matrix. Page 19 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.&86.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 10:02 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 LabiD: C16080582-016 Client Sample 10: E11 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.4 wt% 0.6 mglkg-dry 0.2 pCilg-dry 0.1 pCilg-dry 0.2 pCilg-dry 0.8 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.05 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0,2 D2974 08/15116 10:421 smm 0.03 SW6020 08131116 22:311 sf E909.0 09129116 11 :47 I eli-cs E909.0 09129116 11:47 I eli-cs E909.0 09129116 11:47 I eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -Rl increased due to sample matrix, Page 20 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Colle1a Station, TX 888.890.2218 • Gillette, WY 868 .686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 10:08 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: C16080582-017 Client Sample ID: E12 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.5 wt% 0.1 mglkg-dry 0.5 pCilg-dry 0.2 pCilg-dry 0.2 pCi/g-dry 0.5 pCi/g-dry 0.1 pCi/g-dry 0.04 pCi/g-dry 0.3 pCi/g-dry 0.06 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15/16 10:43/ smm 0.03 SW6020 08/31/16 22:331 sf E909.0 09/29/16 13:30 I eli-cs E909.0 09129/16 13:30 I eli-cs E909.0 09129116 13:30 I eli-cs E903.0 09114116 09:40 I dmf E903.0 09/14/16 09:40 I dmf E903.0 09/14/16 09:40 I dmf E908.0 09/14/16 09:57 I eng E908.0 09/14116 09:57 I eng E908.0 09/14116 09:57 I eng MCL -Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 21 of 70 EN:RGY Trust our People. Trust our Data. www.energyiJb.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.890.2218 • Gillette, WY 866.886.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 10:20 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-018 Client Sample ID: E13 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 1.3 wt% 0.1 mglkg-dry 0.2 pCilg-dry 0.1 pCilg-dry 0.2 pCilg-dry 1.0 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.1 pCilg-dry 0.02 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:431 smm 0.03 SW6020 08131116 22:36/ sf E909.0 09129116 15:13 I eli-cs E909.0 09129116 15:13 I eli-cs E909.0 09129116 15:131 eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 22 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.680.2218 • Gillette, WY 866.886.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Ca.sper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 10:26 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: C16080582-019 Client Sample ID: E14 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.1 mglkg-dry 0.08 pCilg-dry 0.1 pCilg-dry 0.2 pCilg-dry 0.4 pCilg-dry 0.09 pCilg-dry 0.05 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:431 smm 0.03 SW6020 08131116 22:381 sf E909.0 09129116 16:57 I eli-cs E909.0 09129116 16:57 I eli-cs E909.0 09129116 16:57 I eli-cs E903.0 10124116 08:20 I trs E903.0 1 0124116 08:20 I trs E903.0 1 0124116 08:20 I trs E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D-RL increased due to sample matrix. Page 23 of 70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.68&.7175 • Helena, MT 871.472.0711 LAB ORA TORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 10:28 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab 10: c 16080582-020 Client Sample 10: E15 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RAOIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.1 mglkg-dry 1.1 pCilg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.4 pCilg-dry 0.1 pCilg-dry 0.05 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:43 I smm 0.03 SW6020 08131116 22:411 sf E909.0 09129116 18:40 I eli-cs E909.0 09129116 18:40 I eli-cs E909.0 09129116 18:40 I eli-cs E903.0 1 0124116 08:20 I trs E903.0 10124116 08:20 I trs E903.0 10124116 08:20 I trs E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 24 of 70 EN:RGY / Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.688.7175 • Helena, MT 871.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03117 Report Date: 1 0/26/16 Collection Date: 08/09/16 10:33 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-021 Client Sample ID: E16 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.3 mg/kg-dry 0.7 pCi/g-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.4 pCilg-dry 0.08 pCilg-dry 0.03 pCilg-dry 0.3 pCilg-dry 0.06 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15/16 10:44/ smm 0.03 SW6020 09/02/16 15:42 I sf E909.0 09130116 06:41 I eli-cs E909.0 09130/16 06:41/ eli-cs E909.0 09130116 06:41 I eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09/19116 10:00 I dmf E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng E908.0 09114116 14:45/ eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 25 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.wm Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 10:39 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-022 Client Sample ID: E17 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units NO wt% 0.1 mglkg-dry 0.7 pCilg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.3 pCilg-dry 0.08 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.1 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:441 smm 0.03 SW6020 09102116 15:441 sf E909.0 09130116 08:24 I eli-cs E909.0 09130116 08:241 eli-cs E909.0 09130116 08:24 I eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:451 eng E908.0 09/14/16 14:45/ eng E908.0 09114116 14:45/ eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D-RL increased due to sample matrix. Page 26 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 988.890.2218 • Gillette, WY 886.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 10:44 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-023 Client Sample ID: E18 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 0.2 wt% 0.2 mglkg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.3 pCilg-dry 0.08 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.2 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:441 smm O.Q3 SW6020 09102116 16:07 I sf E909.0 09130116 01 :31 I eli-cs E909.0 09130116 01 :31 I eli-cs E909.0 09130116 01:31/ eli-cs E903.0 09119116 10:00 I dmf E903.0 09119/16 10:00 I dmf E903.0 09119/16 10:00 I dmf E908.0 09114116 14:451 eng E908.0 09114116 14:45/ eng E908.0 09/14/16 14:45 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 27 of70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 871.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 10:51 DateReceived: 08112116 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 LabiD: c 16080582-024 Client Sample ID: S01 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Anaiyte reporting limit. QCL-Quality control limit. Result Units NO wt% 0.2 mglkg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.4 pCilg-dry 0.09 pCilg-dry 0.04 pCilg-dry 0.08 pCilg-dry 0.02 pCilg-dry 0.1 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:44 I smm 0.03 SW6020 09102116 16:09 I sf E909.0 09130116 10:07 I eli-cs E909.0 09130116 10:07 I eli-cs E909.0 09130116 10:07 I eii-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng E908.0 09114116 14:45/ eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 28 of70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 86&.&8&.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 08:30 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-025 Client Sample ID: S02 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.08 mglkg-dry 0.7 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.2 pCi/g-dry 0.06 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:44/ smm 0.03 SW6020 09102116 16:121 sf E909.0 09/30116 11:50 I eii-cs E909.0 09130116 11:50 I eli-cs E909.0 09130116 11:50 I eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:45/ eng E908.0 09/14116 14:45/ eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D -Rl increased due to sample matrix. Page 29 of 70 EN:RGY Trust our People. Trust our Data. www.ene1gylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 12:47 DateReceived: 08/12116 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-026 Client Sample ID: S03 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units ND wt% 0.1 mglkg-dry 0.8 pCilg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.05 pCilg-dry 0.04 pCilg-dry 0.3 pCilg-dry 0.05 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:00 I smm 0.03 SW6020 09102116 16:141 sf E909.0 09130116 13:33 I eli-cs E909.0 09130116 13:33 I eli-cs E909.0 09130116 13:331 eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng E908.0 09114/16 14:451 eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 30 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 08:31 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 LabiD: C16080582-027 Client Sample ID: W01 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 0.5 wt% 0.3 mg/kg-dry 0.6 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.6 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.5 pCilg-dry 0.09 pCilg-dry 0.1 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15/16 11:01/ smm 0.03 SW6020 09102116 16:171 sf E909.0 09130116 15:16 I eii-cs E909.0 09130116 15:16 I eii-cs E909.0 09130116 15:16/ eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114/16 14:451 eng E908.0 09114/16 14:451 eng E908.0 09/14/16 14:45/ eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 31 of 70 I Er\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT BOO. 735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 08:38 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-028 Client Sample ID: W02 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units ND wt% 0.3 mg/kg-dry 0.8 pCi/g-dry 0.3 pCi/g-dry 0.2 pCi/g-dry 1 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.3 pCilg-dry 0.06 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15/1611 :01/ smm 0.03 SW6020 09/02/1616:19/sf E909.0 09130116 16:59/ eli-cs E909.0 09/30116 16:59/ eli-cs E909.0 09130/16 16:59 I eli-cs E903.0 09119/16 10:00 I dmf E903.0 09/19/16 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:45 I eng E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 32 of 70 EI\ERGY Trust our People. Trust our Data. www.ene rgylab.(Om Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 08:43 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-029 Client Sample ID: W03 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units ND wt% 0.4 mglkg-dry 1.1 pCilg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.8 pCilg-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 0811511611:011 smm 0.03 SW6020 09102116 16:22 I sf E909.0 09130116 18:42 I eli-cs E909.0 09130116 18:42 I eli-cs E909.0 09130116 18:42 I eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:451 eng E908.0 09114116 14:45 I eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. 0 -RL increased due to sample matrix. Page 33 of70 EI\ERGY •' Trust our People. Trust our Data. www.ene1gylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 08:46 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-030 Client Sample ID: W04 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADION UC Ll DES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 1.8 wt% 0.4 mglkg-dry 2.0 pCilg-dry 0.6 pCilg-dry 0.2 pCilg-dry 0.6 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.05 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15116 11:02 I smm 0.03 SW6020 09102116 16:24 I sf E909.0 09130116 20:261 eli-cs E909.0 09130116 20:261 eli-cs E909.0 09130116 20:26/ eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 34 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.886.7175 • Helena, MT 871.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 13:51 DateReceived: 08/12116 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-031 Client Sample ID: W05 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 2.0 wt% 0.3 mglkg-dry 2.5 pCilg-dry 0.8 pCilg-dry 0.2 pCi/g-dry 0.4 pCilg-dry 0.09 pCilg-dry 0.03 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:021 smm 0.03 SW6020 09102116 16:27 I sf E909.0 09130116 22:091 eli-cs E909.0 09130116 22:091 eli-cs E909.0 09130116 22:091 eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:451 eng E908.0 09114116 14:45 I eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 35 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.tom Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.890.2218 • Gillette, WY 866.886.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 13:47 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-032 Client Sample ID: W06 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 1.4 wt% 0.1 mglkg-dry 0.8 pCilg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.4 pCilg-dry 0.09 pCilg-dry O.Q3 pCilg-dry 0.1 pCilg-dry 0.03 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 11:021 smm 0.03 SW6020 09102116 16:39 I sf E909.0 09130116 23:521 eli-cs E909.0 09130116 23:521 eli-cs E909.0 09130116 23:521 eli-cs E903.0 09119116 12:08 I dmf E903.0 0911911612:081 dmf E903.0 09119116 12:081 dmf E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 36 of70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 888.888.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Dat.e: 08/09/16 12:44 DateReceived: 08/12116 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-033 Client Sample ID: W07 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.1 mg/kg-dry 1.6 pCi/g-dry 0.5 pCi/g-dry 0.2 pCilg-dry 0.3 pCilg-dry O.o? pCilg-dry 0.04 pCilg-dry 0.3 pCilg-dry 0.07 pCilg-dry 0.1 pCilg-dry MDC - Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15/16 11 :03/ smm 0.03 SW6020 09/02/16 16:42/ sf E909.0 10/01/16 01 :35/ eli-cs E909.0 10101116 01 :35 I eli-cs E909.0 10101116 01 :35 I eli-cs E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 37 of70 EN:RGY Trust our People. Trust our Data. www.energylab.(om Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.688.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09116 13:40 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-034 Client Sample ID: wo8 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units ND wt% 0.2 mglkg-dry 1.5 pCilg-dry 0.5 pCilg-dry 0.2 pCilg-dry 0.4 pCilg-dry 0.09 pCi/g-dry 0.03 pCi/g-dry 0.2 pCilg-dry 0.04 pCi/g-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:031 smm 0.03 SW6020 09102116 16:441 sf E909.0 10101116 03:18 I eli-cs E909.0 10101116 03:18 I eli-cs E909.0 10101/16 03:181 eli-cs E903.0 09/19116 12:08 I dmf E903.0 09/19116 12:08 I dmf E903.0 09/19116 12:08 I dmf E908.0 09114116 14:451 eng E908.0 09114/16 14:45/ eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 38 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 13:36 DateReceived: 08/12116 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-035 Client Sample ID: W09 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units ND wt% 0.07 mg/kg-dry 1.2 pCi/g-dry 0.4 pCi/g-dry 0.2 pCi/g-dry 0.2 pCi/g-dry 0.06 pCi/g-dry 0.03 pCi/g-dry 0.2 pCi/g-dry 0.03 pCi/g-dry 0.2 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 02974 08/15/16 11:03 1 smm 0.03 SW6020 09/02/16 16:47 1 sf E909.0 10/01/16 05:01 1 eli-cs E909.0 10/01/16 05:01 1 eli-cs E909.0 10/01/16 05:01 1 eli-cs E903.0 09/19/16 12:081 dmf E903.0 09/19/16 12:08 1 dmf E903.0 09/19/16 12:081 dmf E908.0 09/14/16 14:45 1 eng E908.0 09/14/16 14:45 1 eng E908.0 09/14/16 14:45 1 eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 39 of 70 EN:RGV ' Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 13:33 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-036 Client Sample ID: W10 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.8 wt% 0.1 mg/kg-dry 0.4 pCilg-dry 0.2 pCi/g-dry 0.2 pCi/g-dry 0.4 pCi/g-dry 0.1 pCi/g-dry 0.04 pCi/g-dry 0.4 pCi/g-dry 0.08 pCilg-dry 0.2 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15/16 11:03 I smm 0.03 SW6020 09/02/16 16:49 I sf E909.0 10101116 06:44 I eli-cs E909.0 10/01/16 06:44/ eli-cs E909.0 10/01/16 06:44/ eli-cs E903.0 09/19/16 12:08/ dmf E903.0 09/19/16 12:08/ dmf E903.0 09/19/16 12:08/ dmf E908.0 09114116 14:45 I eng E908.0 09/14116 14:45 I eng E908.0 09/14/16 14:45/ eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 40 of70 Er\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Collage Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26116 Collection Date: 08/09/16 13:13 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab 10: C16080582-037 Client Sample ID: W11 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.2 mglkg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.3 pCilg-dry 0.07 pCilg-dry 0.03 pCilg-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 11 :04 I smm 0.03 SW6020 09102/16 16:521 sf E909.0 10101116 08:27 I eli-cs E909.0 10101116 08:27 I eli-cs E909.0 10101/16 08:27 I eli-cs E903.0 09119/16 12:08 I dmf E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E908.0 09114116 14:451 eng E908.0 09114116 14:45/ eng E908.0 09114116 14:451 eng MCL -Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 41 of70 EI\ERGY ' Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.686.7175 • Helena, MT 817.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 13:16 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-038 Client Sample ID: W12 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.9 wt% 0.08 mg/kg-dry 0.7 pCi/g-dry 0.3 pCi/g-dry 0.2 pCi/g-dry 0.2 pCilg-dry 0.06 pCilg-dry 0.03 pCilg-dry 0.09 pCilg-dry 0.02 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 0811511611:041 smm 0.03 SW6020 09102116 16:541 sf E909.0 10101116 10:10 I eli-cs E909.0 10101116 10:10 I eli-cs E909.0 10101116 10:10 I eli-cs E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E903.0 09119/16 12:081 dmf E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng E908.0 09/14/16 14:45 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -Rl increased due to sample matrix. Page 42 of 70 EN:RGY Trust our People. Trust our Data. www energyiJb.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANAL YTJCAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 13:22 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: C16080582-039 Client Sample ID: W13 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units NO wt% 0.2 mg/kg-dry 0.5 pCi/g-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.3 pCilg-dry 0.07 pCi/g-dry 0.03 pCi/g-dry 0.1 pCilg-dry 0.02 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 02974 08115/16 11:041 smm 0.03 SW6020 09102116 16:57 I sf E909.0 10/01116 11 :53 I eli-cs E909.0 10101116 11:53 I eli-cs E909.0 10101116 11:53 I eli-cs E903.0 09119116 12:08 I dmf E903.0 09119116 12:081 dmf E903.0 09119116 12:081 dmf E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng MCL -Maximum contaminant level. NO-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 43 of70 EI\ERGY •' Trust our People. Trust our Data. www.eoe1yylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.886.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 13:26 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-040 Client Sample ID: W14 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 lead 210 precision (±) lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: Rl-Analyte reporting limit. QCl-Quality control limit. Result Units ND wt% 0.4 mg/kg-dry 0.4 pCi/g-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.002 pCilg-dry 0.02 pCilg-dry 0.03 pCilg-dry 0.4 pCilg-dry 0.07 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11 :04 I smm 0.03 SW6020 09102116 16:591 sf E909.0 10101116 13:361 eli-cs E909.0 10101116 13:361 eli-cs E909.0 10101116 13:36 I eli-cs E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E908.0 09114116 14:461 eng E908.0 09114116 14:461 eng E908.0 09114116 14:461 eng MCl-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 44 of70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 868.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 12:57 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-041 Client Sample ID: W15 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result Units ND wt% 0.4 mg/kg-dry 0.3 pCi/g-dry 0.1 pCilg-dry 0.1 pCi/g-dry 0.2 pCilg-dry 0.06 pCilg-dry 0.03 pCilg-dry -30 pCilg-dry 2610 pCilg-dry 0 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 08115/16 11:05 I smm 0.03 SW6020 09102/16 21:141 sf E909.0 10102116 00:531 eli-cs E909.0 10102116 00:531 eli-cs E909.0 10102116 00:531 eli-cs E903.0 09119116 12:041 dmf E903.0 09119116 12:041 dmf E903.0 09119116 12:041 dmf E908.0 09116116 09:36 I eng E908.0 09116116 09:36 I eng E908.0 09116116 09:361 eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 45 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.886.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/1612:33 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-042 Client Sample ID: W16 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.4 wt% 0.6 mglkg-dry 0.3 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.3 pCilg-dry 0.08 pCilg-dry 0.03 pCilg-dry -0.05 pCilg-dry 4.4 pCilg-dry 0 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:06 I smm 0.03 SW6020 09102116 21:17 I sf E909.0 10102116 02:361 eli-cs E909.0 10102116 02:361 eli-cs E909.0 10102116 02:361 eli-cs E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E908.0 09116116 09:36 I eng E908.0 09116116 09:361 eng E908.0 09116116 09:36 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 46 of70 EN:RGY Trust our Paopla. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 COllege Station, TX 888.890.2218 • Gillette, WY 866.886.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/1612:37 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-043 Client Sample ID: W17 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 0.6 wt% 0.5 mglkg-dry 0.6 pCilg-dry 0.2 pCilg-dry 0.1 pCi/g-dry 0.4 pCi/g-dry 0.09 pCi/g-dry 0.04 pCi/g-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:061 smm 0.03 SW6020 09102116 21:29/ sf E909.0 10101116 20:14 I eli-cs E909.0 10101116 20:141 eli-cs E909.0 10/01116 20:141 eli-cs E903.0 09119116 12:05 I dmf E903.0 09119/16 12:05 I dmf E903.0 09119/16 12:05 I dmf E908.0 09/16/16 09:36/ eng E908.0 09116116 09:36/ eng E908.0 09116/16 09:36/ eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 47 of 70 EN:RGY •' Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 12:42 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-044 Client Sample ID: W18 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.5 mg/kg-dry 0.8 pCi/g-dry 0.2 pCi/g-dry 0.1 pCi/g-dry 0.5 pCi/g-dry 0.1 pCi/g-dry 0.03 pCi/g-dry 0.5 pCi/g-dry 0.09 pCi/g-dry 0.2 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15/1611:11/ smm 0.03 SW6020 09/02/16 21:32/ sf E909.0 10/02/16 04:19 I eli-cs E909.0 10/02/16 04:19/ eli-cs E909.0 10/02/16 04:19/ eli-cs E903.0 09/19/16 12:05/ dmf E903.0 09/19/16 12:05/ dmf E903.0 09/19/16 12:05/ dmf E908.0 09/16/16 09:36/ eng E908.0 09/16/16 09:36/ eng E908.0 09/16/16 09:36/ eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 48 of?O EI\ERGY ' Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.688.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 09 :04 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-045 Client Sample ID: BHV-1 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.2 wt% 0.7 mglkg-dry 0.4 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.5 pCi/g-dry 0.1 pCi/g-dry 0.04 pCi/g-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU Rl QCL Method Analysis Date I By 0.2 D2974 08/15/16 11:121 smm 0.03 SW6020 09102116 21 :44 I sf E909.0 10102116 06:02 I eli-cs E909.0 10102116 06:02 I eli-cs E909.0 10/02/16 06:02 I eli-cs E903.0 09/19/16 12:05/ dmf E903.0 09/19116 12:05/ dmf E903.0 09/19/16 12:05/ dmf E908.0 09116116 09:36 I eng E908.0 09116116 09:361 eng E908.0 09116/16 09:361 eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 49 of 70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.890.2218 • Gillette, WY 866.888.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:42 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-046 Client Sample ID: BHV-2 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units 1.3 wt% 0.4 mglkg-dry 0.2 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.4 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.4 pCilg-dry 0.07 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:121 smm 0.03 SW6020 09102116 21 :47 I sf E909.0 10102116 07:451 eli-cs E909.0 10102116 07:45 I eli-cs E909.0 10102116 07:45 I eli-cs E903.0 09119116 12:051 dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E908.0 09116116 09:361 eng E908.0 09116116 09:36 I eng E908.0 09116116 09:361 eng MCL -Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 50 of 70 EN:RGY ; ' Trust our People. Trust our Data. www energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 888,88&.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:23 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-04 7 Client Sample ID: BHV-3 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units NO wt% 0.8 mglkg-dry 0.9 pCilg-dry 0.3 pCilg-dry 0.1 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 11:12 I smm 0.03 SW6020 09102116 21 :49 I sf E909.0 10102/16 09:28 I eli-cs E909.0 10102116 09:28 I eli-cs E909.0 10102116 09:28 I eli-cs E903.0 09119116 12:051 dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E908.0 09116116 09:361 eng E908.0 09116116 09:36 I eng E908.0 09116116 09:361 eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 51 of 70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings. MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 10:12 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-048 Client Sample ID: BHV-4 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 2.1 wt% 0.3 mglkg-dry 0.09 pCilg-dry 0.09 pCilg-dry 0.1 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.4 pCilg-dry 0.07 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11 :12 I smm 0.03 SW6020 09102/16 21 :52 I sf E909.0 10102116 11 :11 I eli-cs E909.0 10102116 11 :11 I eli-cs E909.0 1010211611 :111eli-cs E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:051 dmf E908.0 09116116 09:361 eng E908.0 09116116 09:361 eng E908.0 09116116 09:36 I eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 52 of 70 EN:RGY Trust our People. Trust our Data. www.energy lab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Colleae Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:54 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab 10: c 16080582-049 Client Sample ID: BHV-5 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 2.1 wt% 0.8 mglkg-dry 0.4 pCi/g-dry 0.2 pCilg-dry 0.1 pCilg-dry 1.2 pCilg-dry 0.2 pCi/g-dry 0.04 pCilg-dry 0.4 pCilg-dry 0.08 pCi/g-dry 0.1 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15/16 11:131 smm 0.03 SW6020 09102116 21:54/ sf E909.0 10102/16 12:54/ eli-cs E909.0 10102116 12:541 eli-cs E909.0 10102116 12:541 eli-cs E903.0 09/19116 12:051 dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E908.0 09/16/16 09:361 eng E908.0 09/16116 09:361 eng E908.0 09/16/16 09:36/ eng MCL-Maximum contaminant level. NO-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 53 of70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Collage Station, TX 888.890.2218 • Gillette, WY 866.686.7115 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 10:05 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-050 Client Sample ID: BHV-6 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 0.7 wt% 1.3 mglkg-dry 0.3 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.8 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.2 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 11:131 smm 0.03 SW6020 09102116 21:59 I sf E909.0 10102116 14:37 I eli-cs E909.0 10102116 14:37 I eli-cs E909.0 10102116 14:37 I eli-cs E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E908.0 09116116 09:361 eng E908.0 09116116 09:36/ eng E908.0 09/16116 09:36 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 54 of 70 EN:RGY .-Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7115 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:21 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 LabiD: C16080582-051 Client Sample ID: BHV-7 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.1 wt% 0.8 mg/kg-dry 0.2 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.8 pCilg-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.5 pCilg-dry 0.09 pCilg-dry 0.2 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15/16 11:13 I smm 0.03 SW6020 09/02/16 22:02 I sf E909.0 10102/16 16:20 I eli-cs E909.0 10/02/16 16:20 I eli-cs E909.0 10102116 16:20 I eli-cs E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E908.0 09116116 09:361 eng E908.0 09116116 09:361 eng E908.0 09/16/16 09:36/ eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 55 of70 EI\ERGY Trust our People. Trust our Data. www.eneryylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.886.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 08:58 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-052 Client Sample ID: BHV-8 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 1.0 wt% 0.2 mglkg-dry 0.08 pCi/g-dry 0.09 pCilg-dry 0.1 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.03 pCilg-dry 0.3 pCilg-dry 0.06 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 08115/1611:13/ smm 0.03 SW6020 09102116 22:04 I sf E909.0 10102116 18:03 I eli-cs E909.0 10/02116 18:03 I eli-cs E909.0 10102116 16:031 eli-cs E903.0 09119116 14:191 dmf E903.0 · 09119116 14:191 dmf E903.0 09119116 14:191 dmf E906.0 09116116 09:36 I eng E906.0 09116116 09:361 eng E908.0 09116116 09:361 eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 56 of70 EI\ERGY •' Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.890.2218 • Gillette, WY 866.886.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 10:02 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-054 Client Sample ID: E65 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 1.0 wt% 0.4 mglkg-dry 0.2 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.7 pCilg-dry 0.1 pCilg-dry 0.03 pCilg-dry 0.1 pCilg-dry 0.02 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:141 smm 0.03 SW6020 09102116 22:191 sf E909.0 10102116 21 :29 I eli-cs E909.0 10102116 21 :29 I eli-cs E909.0 10102116 21 :291 eli-cs E903.0 09119116 14:19 I dmf E903.0 09119116 14:191 dmf E903.0 09119116 14:191 dmf E908.0 09116116 09:361 eng E908.0 09116116 09:361 eng E908.0 09116116 09:361 eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 58 of70 E~RGY ~ I Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.680.2218 • Gillette, WY 866.888.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 13:51 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-055 Client Sample ID: W70 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units 3.4 wt% 0.2 mglkg-dry 0.3 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.6 pCilg-dry 0.1 pCilg-dry 0.03 pCilg-dry 0.4 pCilg-dry 0.08 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 0811511611:151smm 0.03 SW6020 09102116 22:22 I sf E909.0 10102116 23:12 I eli-cs E909.0 10102116 23:121 eli-cs E909.0 10102116 23:121 eli-cs E903.0 09119116 14:191 dmf E903.0 09119116 14:191 dmf E903.0 0911911614:191dmf E908.0 09116116 09:36 I eng E908.0 09116/16 09:361 eng E908.0 09116116 09:361 eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 59 of70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 86&.&8&.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 08:30 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-056 Client Sample ID: S75 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units NO wt% 0.09 mglkg-dry 0.1 pCi/g-dry 0.1 pCi/g-dry 0.1 pCi/g-dry 0.3 pCi/g-dry 0.06 pCi/g-dry 0.04 pCi/g-dry 0.2 pCi/g-dry 0.04 pCi/g-dry 0.2 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 02974 08/15/16 11 :15/ smm 0.03 SW6020 09/02/16 22:24/ sf E909.0 10/03/16 00:55 I eli-cs E909.0 10/03/16 00:55/ eli-cs E909.0 10/03/16 00:55 I eli-cs E903.0 09/19/16 14:19/ dmf E903.0 09/19/16 14:19/ dmf E903.0 09/19/16 14:19/ dmf E908.0 09/16/16 09:36/ eng E908.0 09/16/16 09:36/ eng E908.0 09/16/16 09:36/ eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. 0 -RL increased due to sample matrix. Page 60 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 88&.&88.7175 • Helena, MT 877.472.0711 CLIENT: Project: Work Order: Energy Fuels Resources (USA) Inc Annual Soils 2016 C16080582 REVISED/SUPPLEMENTAL REPORT Revised Date: 02/03/17 Report Date: 10/26/16 CASE NARRATIVE The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on 1/31/2017 for the addition of Th232 that was requested on the chain of custody. Sample(s) were initially logged and reported as Th230. The data presented here is from that recheck/additional analysis. The report has been revised and replaces any previously issued report in its entirety. BRANCH LABORATORY SUBCONTRACT ANALYSIS Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4•c (±2.C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has. begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-cs -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify Ell's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 4 of70 EN:RGY Trust our People. Trust our Data. www.energylau.com Billings, MT 800.735.4488 • Casper, WV 888.235.0515 College Station, TX 888.880.2218 • Gillette, WV 888.888.7175 • Helena, MT 877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Work Order: C16080582 Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Analyte Method: E903.0 Lab 10: LCS1-48176 Radium 226 Lab 10: MB-48176 Radium 226 Radium 226 precision (±) Radium 226 MDC LabiD: C16080582-001 AMS1 Radium 226 Lab 10: C 16080582-001 AMS 1 Radium 226 Method: E903.0 Lab 10: LCS1-48199 Radium 226 Lab 10: MB-48199 Radium 226 Radium 226 precision (±) Radium 226 MDC LabiD: C16080582-021AMS1 Radium 226 LabiD: C16080582-021AMS1 Radium 226 Method: E903.0 Lab 10: LCS1-48176 Radium 226 Lab 10: MB-48176 Radium 226 Radium 226 precision (±) Radium 226 MDC Lab 10: C16080582-001AMS1 Radium 226 LabiD: C16080582-001 AMS1 Radium 226 Qualifiers: RL -Analyte reporting limit. Count Result Units Laboratory Control Sample 1.5 pCi/g-dry 3 Method Blank 0.01 pCi/g-dry 0.007 pCi/g-dry 0.009 pCi/g-dry Sample Matrix Spike 1.8 pCi/g-dry Sample Matrix Spike Duplicate 1.6 pCi/g-dry Laboratory Control Sample 1.4 pCi/g-dry 3 Method Blank 0.005 pCi/g-dry 0.005 pCi/g-dry 0.008 pCi/g-dry Sample Matrix Spike 1. 7 pCi/g-dry Sample Matrix Spike Duplicate, 1.6 pCi/g-dry Laboratory Control Sample 0.3 pCi/g-dry 3 Method Blank 0.007 pCi/g-dry 0.006 pCi/g-dry 0.009 pCi/g-dry Sample Matrix Spike 1. 7 pCi/g-dry Sample Matrix Spike Duplicate 1. 7 pCi/g-dry MDC-Minimum detectable concentration RL %REC Low Limit High Limit Run:G5000VV_160908B 95 80 120 Run:G5000VV_160908B Run:G5000VV_160908B 84 70 130 Run:G5000VV_160908B 73 70 130 Run:G5000VV_160909A 93 80 120 Run: G5000VV_160909A Run: G5000VV_160909A 84 70 130 Run: G5000VV_160909A 77 70 130 Run: G5000VV_161014B 102 80 120 Run: G5000VV_161014B Run: G5000VV_161014B 79 70 130 Run: G5000VV_161014B 82 70 130 ND-Not detected at the reporting limit. RPD RPDLimit Qual 10.0 6.7 0.4 Batch: 48176 09/14/16 07:44 09/14/16 07:44 09/14/16 07:44 09/14/16 07:44 49.8 Batch: 48199 09/19/1610:00 09/19/16 10:00 u 09/19/16 10:00 09/19/16 10:00 49.7 Batch: 48176 10/24/16 08:20 1 0/24/16 08:20 u 10/24/16 08:20 10/24/16 08:20 20 U -Not detected at minimum detectable concentration Page 61 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 o Casper, WY 888.235.0515 College Station, TK 888.890.2218 o Gillette, WY 88&.&86.7175 o Helena, MT 877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Work Order: C16080582 Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Analyte Method: E903.0 Lab ID: LCS1-48230 Radium 226 Lab ID: MB-48230 Radium 226 Radium 226 precision (±) Radium 226 MDC LabiD: C16080582-041AMS1 Radium 226 Lab ID: C16080582-041AMS1 Radium 226 Qualifiers: RL -Analyte reporting limit. Count Result Units 3 Laboratory Control Sample 1.4 pCilg-dry Method Blank 0.006 pCi/g-dry 0.005 pCi/g-dry 0.008 pCilg-dry Sample Matrix Spike 1.6 pCi/g-dry Sample Matrix Spike Duplicate 1. 7 pCi/g-dry MDC -Minimum detectable concentration RL %REC Low Limit High Limit Run: G542M_160909A 91 80 120 Run: G542M_160909A Run: G542M_160909A 85 70 130 Run: G542M_160909A 94 70 130 ND -Not detected at the reporting limit. RPD RPDLimit Qual 8.7 Batch: 48230 09/19/16 12:04 09/19/16 12:04 u 09/19/16 12:05 09/19/16 12:05 49.6 U -Not detected at minimum detectable concentration Page 62 of70 EI\ERGY Trust our People. Trust our Data. www.ener9ylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Col lei& Station, TX 888.890.2218 • Gillette, WY 888.888.7175 • Helena, MT 877.472.0711 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Work Order: C16080582 Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Analyte Method: E908.0 Lab ID: LCSS-48176 Thorium 230 Lab ID: C16080582-005AMS5 Thorium 230 LabiD: C16080582-005AMS5 Thorium 230 Lab ID: MB-48176 Thorium 230 Thorium 230 MDC Thorium 232 precision (±) Method: E908.0 Lab ID: C16080582-024AMS5 Thorium 230 Lab ID: C16080582-024AMS5 Thorium 230 Count Result Units Laboratory Control Sample 2.3 pCi/g-dry Sample Matrix Spike 3.6 pCi/g-dry Sample Matrix Spike Duplicate 3.5 pCi/g-dry 3 Method Blank 0.002 pCi/g-dry 0.01 pCi/g-dry 0.006 pCi/g-dry Sample Matrix Spike 2.5 pCi/g-dry Sample Matrix Spike Duplicate 2.0 pCi/g-dry RL %REC Low Limit High Limit RPD RPDLimit Qual Batch: 48176 Run: EGG-ORTEC_160907B 09/14/16 09:57 90 80 120 Run: EGG-ORTEC_160907B 09/14/16 09:57 118 70 130 Run: EGG-ORTEC_160907B 114 70 130 2.8 09/14/16 09:57 48 Run: EGG-ORTEC_160907B Run: EGG-ORTEC_160909A 90 70 130 Run: EGG-ORTEC_160909A 69 70 130 24 09/14/16 09:57 u Batch: 48199 09/14/16 14:45 09/14/16 14:45 48.1 s -Spike response is outside of the acceptance range for this analysis. Since the LCS and the RPD recoveries are acceptable, the response is considered to be matrix related The batch is approved. Lab ID: MB-48199 Thorium 230 Thorium 230 MDC Thorium 232 precision (±) Lab ID: LCSS-48199 Thorium 230 Method: E908.0 Lab ID: LCSS-48230 Thorium 230 3 Method Blank 0.003 pCi/g-dry 0.01 pCi/g-dry 0.006 pCi/g-dry Laboratory Control Sample 5.3 pCi/g-dry Laboratory Control Sample 6.4 pCi/g-dry Run: EGG-ORTEC_160909A Run: EGG-ORTEC_160909A 106 80 120 Run: EGG-ORTEC_160912A 128 80 120 -LCS response is outside of the acceptance range for this analysis. Since the MB, MS. and MSD are acceptable the batch is approved. Lab ID: C16080582-044AMS5 Thorium 230 Lab ID: C16080582-044AMS5 Thorium 230 Lab ID: MB-48230 Thorium 230 Thorium 230 MDC Thorium 232 precision (±) Qualifiers: RL -Analyte reporting limit. Sample Matrix Spike 4.1 pCi/g-dry Sample Matrix Spike Duplicate 5.0 pCi/g-dry 3 Method Blank 0.006 pCi/g-dry 0.02 pCi/g-dry 0.008 pCi/g-dry MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration Run: EGG-ORTEC_160912A 77 70 130 Run: EGG-ORTEC_160912A 95 70 130 20 Run: EGG-ORTEC_160912A NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. 09/14/16 14:46 u 09/14/16 14:46 Batch: 48230 09/16/16 09:36 s 09/16/16 09:36 09/16/16 09:36 48 09/16/16 09:36 u Page 63 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 o Casper, WY 888.235.0515 Colla&e Station, TX 888.890.2218 o Gillette, WY 888.888.7175 o Helena, MT 877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Revised Date: 02/03/17 Client: Energy Fuels Resources (USA) Inc Report Date: 10/26/16 Project: Annual Soils 2016 Work Order: C16080582 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimlt Qual Method: E909.0 Batch: T_25516 LabiD: MB-25516 3 Method Blank Run: SUB-T69878 09/28/16 03:08 Lead 210 0.09 pCi/g-dry u Lead 210 precision(±) 0.1 pCi/g-dry Lead 210 MDC 0.2 pCi/g-dry Lab ID: LCS3-25516 Laboratory Control Sample Run: SUB-T69878 09/28/16 04:52 Lead 210 2.2 pCi/g-dry 89 80 120 LabiD: C16080582-003A Sample Matrix Spike Run: SUB-T69878 09/28/16 08:18 Lead 210 2.6 pCi/g-dry 84 70 130 LabiD: C16080582-003A Sample Matrix Spike Duplicate Run: SUB-T69878 09/28/16 10:01 Lead 210 2.7 pCi/g-dry 89 70 130 4.0 71 .1 Method: E909.0 Batch: T_25517 LabiD: MB-25517 3 Method Blank Run: SUB-T69893 09/29/16 22:05 Lead 210 0.09 pCi/g-dry u Lead 210 precision (±) 0.1 pCi/g-dry Lead 210 MDC 0.2 pCi/g-dry LabiD: LCS3-25517 Laboratory Control Sample Run: SUB-T69893 09/29/16 23:48 Lead 210 1.4 pCi/g-dry 53 80 120 s -LCS response is outside of the acceptance range for this analysis. Since the MB, MS, and MSD are acceptable the batch is approved. LabiD: C16080582-023A Sample Matrix Spike Run: SUB-T69893 09/30/16 03:15 Lead 210 2.8 pCi/g-dry 103 70 130 LabiD: C16080582-023A Sample Matrix Spike Duplicate Run: SUB-T69893 09/30/16 04:58 Lead 210 2.4 pCi/g-dry 87 70 130 15 71 .8 Method: E909.0 Batch: T _25550 Lab ID: MB-48230 3 Method Blank Run: SUB-T69894 10/01/16 16:48 Lead 210 0.02 pCi/g-dry u Lead 210 precision(±) 0.09 pCi/g-dry Lead 210 MDC 0.1 pCi/g-dry LabiD: LCS3-48230 Laboratory Control Sample Run: SUB-T69894 10/01/16 18:31 Lead 210 2.2 pCi/g-dry 90 80 120 LabiD: C16080582-043A Sample Matrix Spike Run: SUB-T69894 10/01/16 21 :57 Lead 210 3.4 pCi/g-dry 120 70 130 Lab ID: C16080582-043A Sample Matrix Spike Duplicate Run: SUB-T69894 10/01/16 23:27 Lead 210 3.6 pCi/g-dry 127 70 130 3.8 69.8 Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits. U -Not detected at minimum detectable concentration Page 64 of 70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette. WY 888.888.7175 • Helena. MT877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Work Order: C 16080582 Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Analyte Count Result Method: SW6020 Units RL %REC Low Limit High Limit RPD RPDLimit Qual Analytical Run: ICPMS2-C_160831A LabiD: ICV Initial Calibration Verification Standard 08/31/16 16:01 Uranium 0.0482 mg/L 0.00030 96 90 110 Lab ID: ICSA Interference Check Sample A 08/31/16 16:04 Uranium 0.000182 mg/L 0.00030 Lab ID: ICSAB Interference Check Sample AB 08/31/16 16:06 Uranium 1.20E-05 mg/L 0.00030 Method: SW6020 Batch: 48176 Lab ID: MB-48176 Method Blank Run: ICPMS2-C_160831A 08/31/16 21:26 Uranium 0.007 mg/kg 0.0008 Lab ID: LCS2-48176 Laboratory Control Sample Run: ICPMS2-C_160831A 08/31/16 21:29 Uranium 0.47 mg/kg 0.010 93 75 125 Lab ID: C16080582-020AMS2 Sample Matrix Spike Run: ICPMS2-C_160831A 08/31/16 22:46 Uranium 2.0 mg/kg-dry 0.026 94 75 125 Lab ID: C16080582-020AMSD Sample Matrix Spike Duplicate Run: ICPMS2-C_160831A 08/31/16 22:48 Uranium 1.4 mg/kg-dry 0.026 61 75 125 s Qualifiers: RL -Ana lyle reporting limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits. Page 65 of70 EN:RGY Trust our People. Trust our Data. www.energylab.com -------" Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Collei& Station, TX 888.890.2218 • Gillette, WY 888.688.7175 • Helena, MT 877.472.0711 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Work Order: C16080582 Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Analyte Count Result Method: SW6020 Units RL %REC Low Limit High Limit RPD RPDLimlt Qual Analytical Run: ICPMS2-C_160902A LabiD: ICV Initial Calibration Verification Standard 09/02/16 12:26 Uranium 0.0483 mg/L Lab ID: ICSA Interference Check Sample A Uranium 0.000173 mg/L Lab ID: ICSAB Interference Check Sample AB Uranium 1.66E-05 mg/L Method: SW6020 Lab ID: MB-48199 Method Blank Uranium ND mg/kg LabiD: LCS2-48199 Laboratory Control Sample Uranium 1.1 mg/kg LabiD: C16080582-022ADI L Serial Dilution Uranium ND mg/kg-dry Lab ID: C16080582-022AMS2 Sample Matrix Spike Uranium 1.2 mg/kg-dry Lab ID: C16080582-040ADI L Serial Dilution Uranium 0.26 mg/kg-dry Method: SW6020 LabiD: MB-48230 Method Blank Uranium 0.02 mg/kg LabiD: LCS2-48230 Laboratory Control Sample Uranium 1.1 mg/kg LabiD: C16080582-042ADI L Serial Dilution Uranium 1.9 mg/kg-dry Lab ID: C16080582-042AMS2 Sample Matrix Spike Uranium 1.4 mg/kg-dry Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration S-Spike recovery outside of advisory limits. 0.00030 97 90 110 0.00030 0.00030 Run: ICPMS2-C_160902A 0.0008 Run: ICPMS2-C_1 60902A 0.010 110 75 125 Run: ICPMS2-C_160902A 0.13 Run: ICPMS2-C_160902A 0.026 89 75 125 Run: ICPMS2-C_160902A 0.13 Run: ICPMS2-C_160902A 0.0008 Run: ICPMS2-C_160902A 0.010 110 75 125 Run: ICPMS2-C_160902A 0.13 Run: ICPMS2-C_160902A 0.026 67 75 125 ND -Not detected at the reporting limit. R -RPD exceeds advisory limit. 09/02/16 12:28 09/02/16 12:31 Batch: 48199 09/02/16 15:35 09/02/16 15:37 09/02/16 15:47 10 09/02/16 15:49 09/02/16 17:12 43 10 R Batch: 48230 09/02/16 20:57 09/02/16 20:59 09/02/16 21:19 110 10 R 09/02/16 21:22 s Page 66 of 70 EN:RGY Trust our People. Trust our Data. www.energylab com Work Order Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Tessa Parke Reviewed by: Tessa Parke Reviewed Date: 8/12/2016 Shipping container/cooler in good condition? Custody seals intact on all shipping container(s)/cooler(s)? Custody seals intact on all sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.) Temp Blank received in all shipping container(s)/cooler(s)? Container/Temp Blank temperature: Water-VOA vials have zero headspace? Water-pH acceptable upon receipt? Standard Reporting Procedures: Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes D ac Yes D Yes D Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Gillette, WY 888.888.7175 • Helena, MT 877.472.0711 C16080582 Date Received: 8/12/2016 Received by: dcj NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD Carrier name: Next Day Air Not Present D Not Present D Not Present 0 Not Applicable 0 No VOA vials submitted 0 Not Applicable 0 Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Contact and Corrective Action Comments: None Page 67 of 70 Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: Energy Laboraties Contact: Garrin Palmer --:;2~39::-:3~S!:-a"'7.1t:-'-'C~r..;.;ee~k~H"":-wy-.-------Ph: 435 678 2221 Casper WY, 82601 gpalmer@energvfuels.com Chain of Custody/Sampling Analysis Request Project Samplers Name Samplers Signature Annual Soils 2016 Garrin Palmer I 6~~ Time Sample ID Date Collected Collected Laboratory Analysis Requested N01 8/9/2016 826 Radlum-226, Pb-210, Th-232, U-nat N02 8/9/2016 852 Radium-226, Pb-210 Th-232, U-nat N03 8/9/2016 854 Radium-226, Pb-21 0, Th-232, U-nat N04 8/9/2016 901 Radium-226, Pb-210, Th-232, U-nat NOS 8/9/2016 902 Radium-226, Pb-21 0, Th-232, U-nat E01 8/9/2016 908 Radium-226, Pb-210, Th-232, U-nat E02 8/9/2016 912 Radium-226, Pb-21 o, Th-232, U-nat E03 8/9/2016 916 Radium-226, Pb-210, Th-232, U-nat E04 8/9/2016 918 Radium-226, Pb-210, Th-232, U-nat E05 8/9/2016 923 Radium-226, Pb-21 o, Th-232, U-nat E06 8/9/2016 927 Radium-226, Pb-210, Th-232, U-nat E07 8/9/2016 930 Radium-226, Pb-21 0, Th-232, U-nat EOB 8/9/2016 951 Radium-226, Pb-210, Th-232, U-nat E09 8/9/2016 956 Radium-226, Pb-21 0, Th-232, U-nat E10 8/9/2016 959 Radium-226, Pb-210, Th-232, U-nat E11 8/9/2016 1002 Radium-226, Pb-21 0, Th-232, U-nat E12 8/9/2016 1008 Radium-226, Pb-21 0, Th-232, U-nat E13 8/9/2016 1020 Radium-226, Pb-210, Th-232, U-nat Comments: Please send report to Kathy Weinel at kweinel@energytuels.com RBin&::Sigb'"~ Date/Time Received By:(Signature) Date/Time 8/10/2016 1230 Relinquished By:(Signature) Date/Time Received By:(Signature) gJj~ .......... ~ '-1. ~ ...... ~ -//liD • -.-. -A _... Samples Shipped to: Project Annual Soils 2016 Sample 10 E14 E15 E16 E17 E18 S01 S02 S03 W01 W02 W03 W04 W05 W06 W07 Wo8 W09 W10 . ~-·· -.·· .-·-Sheet 1 of 1 CHAIN OF CUSTODY ~E~n~er~g~y...;;:L~a=bo;.;.r.;;;.at~ie~s:---------Contact: Garrin Palmer 2393 Salt Creek Hwy. Ph: 435 678 2221 Casper WY, 82601 gpalmer@energyfuels.com Chain of Custody/Sampling Analysis Request Samplers Name Samplers Signature Garrin Palmer I G~ p)A ... Time Date Collected Collected Laborato_ry Analysis Requested 8/9/2016 1026 Radlum-226 Pb-21 0, Th-232, U-nat 8/9/2016 1028 Radium-226, Pb-210, Th-232, U-nat 8/9/2016 1033 Radium-226, Pb-21 0, Th-232, U-nat 8/9/2016 1039 Radium-226, Pb-21 0, Th-232, U-nat 8/9/2016 1044 Radlum-226, Pb-210, Th-232, U-nat 8/9/2016 1051 Radium-226, Pb-210 Th-232, U-nat 8/10/2016 830 Radlum-226, Pb-210, Th-232, U·nat 8/9/2016 1247 Radium-226, Pb-21 0, Th-232, U-nat 8/9/2016 831 Radium-226, Pb-210, Th-232, U-nat 8/9/2016 838 Radium-226, Pb-210, Th-232, U-nat 8/9/2016 843 Radium-226, Pb-210, Th-232, U-nat 8/9/2016 846 Radlum-226 Pb-21 0, Th-232, U-nat 8/9/2016 1351 Radium-226, Pb-21 0, Th-232, U-nat 8/9/2016 1347 Radlum-226, Pb-21 0, Th-232, U-nat 8/9/2016 1244 Radium-226, Pb-21 0, Th-232, U-nat 8/9/2016 1340 Radium-226, Pb-21 0, Th-232, U-nat 8/9/2016 1336 Radlum-226, Pb-210, Th-232, U-nat 8/9/2016 1333 Radium-226, Pb-210, Th-232, U-nat Comments: Please send report to Kathy Weinel at kweinel@ energyfuels.com Datemme Received By:(Signature) 8/10/2016 1230 Datemme Received By:(Signature) Datemme Date/Time ··' Sheet 1 of 1 .. , CHAIN OF CUSTODY Samples Shipped to: Energy Laboraties Contact: Garrin Palmer ~2~39:::3~S~a~lt=:C=..:.re-=e:::;.;::k~H-wy-.-------Ph: 435 678 2221 Casper WY, 82601 gpalmer@enerqvtuels.com Chain of Custody/Sampling Analysis Request Project Sampler• Name Samplers Signature Annual Solis 2016 Garrin Palmer I G.x~·-~ Time SampleiD Date Collected Collected laboratory Analysis Requested E65 8/9/2016 1002 Radium-226, Pb-21 0, Th-232, U-nat W70 8/9/2016 1351 Aadlum-226, Pb-210, Th-232, U-nat S75 8/10/2016 830 Radium-226, Pb-210, Th-232, U-nat Comments: Please send report to Kathy Weinel at kweinel@energyfuels.com Relinquished By:(Signature~ Date/Time Received By:(Signature) Date/Time ~-8/10/2016 1230 Relinquished By:(Signature) Date/Time Received By:(Signature) Date/Time ATTACHMENT I SOIL SAMPLE GRAPHS, DATA TABLE, LABORATORY RESULTS AND QNQC 11 12 07 08 09 BHV-2 10 11 • 13 18 17 16 15 14 14 w w ,t; N 0:: ~ N01 NO. N03 N04 N 5 23 24 19 20 ""' i\ \21 \ BHV 1 22 23 ·r E01 W01 ...-.• "'L E02 --BHV-8 -~E03 W02 ..--lJ BHV_l..t. 1.----E04 W03 ~ r Eos 26 25 30 29 28 27 26 W04 E06 _.lJr E07 BHV~" E08 vyos ... ~ E09 wp6-E10 BHV. 35 36 31 W07 32 33 34 E11 35 wog wo1~ ~ BHV-~ L.---_E12 "' ' • BHV-4 T37S ~E13 T38S W10/. 01 06 05 04 k "' 02 02 ~ 14 W11/. Ene1gy Fuels Resour es (USA) Inc. v )'r \ E15 W12 W13 1 W14 12 07 09 r--'0 11 11 W15-08 , / E16 W16 1 W17/ r---E17 '\ r\· i 14 13 18 17 / 16 r--15 N ~ W18 E18 ... 11N~ : ... L MI.I .. IZS ,._ ~ s12 \S03 ~ 1 0.5 0 1 I 1\i iles S01 l~ 19 20 21 22 2( ..\ Legend ~ Proposed Soil Monitoring Location i * 1,000 Feet * 2,500 Feet ''llf, ENERGYFUELS + Air Monitoring Station REVISIONS Project: WHITE MESA MILL ~ Date: By: County: San Juan State: Utah i =Property Boundary location:- --Road FIGURE 1-1 0 Township and Range O section Coordinate System: NAD SOIL MONITORING LOCATIONS ~ 1983 StatePiane Utah ~ South FIPS 4303 Feet Author: rellis I Date: 2120/2017 I Drafted By: rellis !=' ...... 1\:) ~ 0 01 ..... (n 1\:) (n w 01 Jul-98 Jan-99 Jul-99 Jan-00 Jul-00 Jan-01 + Jul-01 Jan-02 OJ I Jul-02 < I ...... Jan-03 + Jul-03 liJ OJ Jan-04 ::r:: I < < Jul-04 ::rJ I 1\) D) + Jan-05 c. Jul-05 c OJ 3 I Jan-06 I < !\) I !\) c.> Jul-06 -0) + Jan-07 0 0 :I OJ Jul-07 n I CD < Jan-08 :I .j.. -., + Jul-08 D) !:!'. Jan-09 0 OJ :I I Jul-09 en < -I Jan-10 :I 01 + CJ) Jul-1 0 2. 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I <I LO ,... 0 0 ,... 0 LO 0 0 - 0 0 0 9~-onv 9 ~-1nr CXl ,... ~ 9~-unr f. ,.._ ,... 9 ~-keV'J ~ t co ,... 9~-JdV ~ t 1.() 9 ~ -JBV\J ,... ~ + 9 ~-qa.:J """ ,... ~ + 9~-uer C') ,... I 3: g~-oaa + C\1 ,... ~ S~·AON + ,... ,... ~ S~·PO + 0 ,... I 3: g~-das + g~-onv -~ 0 c. --·s en c -f/) c 0 ... m """ -c CD () c 0 0 0 ,.... N I .c D. > J: m C\J 0 0 9~-Bnv 9~-1nr CX) > I Ill 9~-unr t I'-> I Ill 9 ~-ABV\1 t co > 9 ~ -Jd\f I Ill + 10 9 ~ -JBV\1 > I Ill + 9~-qa.:1 '<t I > I Ill 9~-uer + (") > I Ill s~-oaa + C\1 > I S~-AON Ill + .- S~-PO > I Ill + s~-das s~-Bnv -~ 0 a. -·a en c 1/) c 0 -.:; cu ... -c Q) u c 0 0 0 ...... N I Jl ll. ..c -::l 0 en "D c cu ..c t: 0 z 0 "! 8 .,.... 0 co 0 0 co 0 0 '<t 0 0 "! 0 0 0 0 9 ~-5nv 9klnr C') 0 ch 9~-unr f C\J 0 ch 9 ~-ABV'J t ..... 0 9 ~ -Jd'v' ch + 10 9 ~-JBV'J 0 z + 9 ~-qa.:J '<t 0 ' z 9 ~-uer + C') 0 z g~-oaa + C\J 0 ' z g~-AON + ..... S~-PO 0 z + g~-das g ~ -5nv -~ 0 c. --·s U) c -(/) c 0 :;::::; cu ... -c Cl) (.) c 0 0 0 """ N I Jl c.. -m 0 I w """ 0 I w --(/) cu w 0 L!') C') 0 0 cr) 0 L!') C\J 0 0 C\J 0 L!') 0 L!') 0 0 0 0 9 ~ -onv 9~-1nr 9~-unr 9~-Ae~ 9 ~ -Jdy 9~-Je~ 9 ~-qa.:1 9~-uer g~-oaa g~-AON 9~-PO g~-das s ~ -onv Ol 0 w f IX) 0 w f 1'-0 I w t co 0 w + I!) 0 w + ;g w + C') 0 w + C\1 0 I w + ..-0 w + -!f 0 a. --·s C/) c -tn c 0 ; cu ... -c Q) CJ c 0 0 0 .... N I .a Q. -co .... I w 0 .... I w --tn cu w 0 0 cv:i 0 I{) C\1 0 0 C\i 0 I{) 0 0 0 I{) c) 0 0 c) 9~-Bnv 9~-1nr 9 ~-unr 9 ~-ABV\1 9~-JdV 9 ~ -JBV\1 9 ~-qa.::1 9 ~-uer 9~-oaa 9~-AON 9~-PO 9~-das 9~-Bnv co w t ,..._ ~ w f co ~ w t LO ~ w + '<t ~ I UJ + (") ~ w + C\J ~ I UJ + ~ w + 0 .-w + 9 ~ -onv 9~-1nr 0) 0 ~ 9~-unr t -~ co 0 0 c. 9 ~-ABV'J ~ -f ·c; en c 1'-0 rn 9 ~ -Jd'v' ~ c t 0 ; ca ... -co c 9 ~-JBV'J 0 CD ~ u c + 0 0 0 9 ~-qa.:J 10 ,.... 0 N ~ I .c + D.. -(7) 0 9~-uer "<t I == 0 ~ ,.... + 0 I 9~-::>ao == -C') -0 rn ~ CD + == 9~-AON N 0 I s: 9~-PO + ..... 0 I s: 9~-das + 9 ~ -onv 0 0 0 0 0 0 0 0 1./) 0 ~ ~ 1./) 0 cr) C\i C\J ..... c) 0 9~-onv 9~-1nr co ,.... ~ 9~-unr f -~ r-... 0 ,.... I c. 9 ~-AeV'J $: --~ ·a Cl) c CD -0 9~-JdV ~ c 0 t ·.;: «1 ... -1.() c CD 9 ~-J'BV'J ~ (.) c f 0 0 0 '<t ,.. 9 ~-qa.:J ,.... C\1 ~ I Jl + 0.. -co ,.. 9~-uer I (") == ,.... ~ 0 + ,.. ;: 9~-~aa -(\J -,.... I 0 $: ~ + 9~-AON ..... I $: 9~-PO + 0 ..... I $: g~-das + g ~-onv 0 0 0 0 0 0 0 0 ""': "! ~ <X) co "<t C\1 0 ,-0 0 0 0 0 9 ~ -onv 9~-1nr co > I Ill 9~-unr f 1'-> I Ill 9 ~ -liBIN t co > 9 ~ -JdV I -Ill ~ + 0 Q. -lO 0 9 ~-JBIN > en I Ill c + UJ c 0 9~-qa.:J '<t +:: > cu a.. I -Ill c + Cl) (.) 9~-uer c 0 (.) C') > N I ('I) Ill N g~-oaa + I .t:. 1-> C\1 :I: I m > I g~-AON Ill + ,..- 9 ~-PO > I Ill + g~-das g ~ -onv -!? (.) a. -·s en c -U) c 0 :,;::; ca ... -c C1) u c 0 (.) N ('I) N I .c 1- .c -:::s 0 en "C c ca .c t:: 0 z 0 r--. 0 0 <D 0 0 "<t 0 0 C') 0 0 (\J 0 0 ..... 0 0 0 0 9 ~ -5nv 9~-1nr C') 0 ch 9~-unr { C\J 0 ch 9 ~-kBV'J t T""" 0 9 ~ -Jd'v' ch + 10 9 ~-JBV\1 0 z + 9~-qa.:J '<t 0 I z 9~-uer + C') 0 z Skoaa + C\J 0 I z g ~-AON + T""" S~-PO 0 I z + g~-das s ~ -5nv -~ 0 c. -·c; (/) c w c 0 ~ -c CD (,) c 0 (.) N C") ~ .c 1--0) 9 w T"' 0 I w --w co w lO C") 0 -~ lO C\1 0 ~ 0 C\1 0 lO 0 0 0 lO 0 0 - 0 0 0 9~-onv 9~-1nr CJ) 0 9~-unr I w t co 9 ~-keV\1 0 w t 9 ~-JdV " 0 w t 9 ~ -JEV\1 <D 0 I w + 9~-qa.:J LO 0 I w + 9~-uer '<t 0 w + g~-oaa C') 0 w + g~-AON C\J 0 w 9~-PO + ,.... 0 w g~-das + g~-onv -~ 0 Q. --·o C/) c t/J c 0 ;: l! -c Q) (J c 0 (.) N C') ~ .z:: t--co ,... I w 0 ,... I w --t/J cu w 10 """ c) ~ 0 """ c) \ 0 C") c) \ 10 C\1 c) -< 0 C\1 c) \ . ~ 1.0 0 ..-..- c) c) 1.0 0 c) 0 0 c) 9 ~ -5nv 9~-1nr 9~-unr 9 ~-ABV\1 9 ~ -Jd'v' 9 ~ -JBV\1 9 ~-qa.:J 9~-uer 9~-oaa g~-AON 9~-PO g~-das g ~-5nv co ...-I UJ ~ I'-..... w f CD w t 1.0 ...-w + '<t ...-w + C') ..... w + C\J ..... w + ..... w + 0 ..... w + 9~-onv 9~-1nr Ol 0 I s: 9~-unr t -C) :":::: co 0 0 c. 9 ~-ABV\1 ~ -f -'() (/) c:: r-. -0 , 9~-Jd\f ~ c:: t 0 ·.;:: «< a.. -co c:: 9 ~ -JBV\1 0 C1) ~ (,) c:: + 0 0 C\1 9 ~-qa.:J 1.{) M 0 ~ ~ .c + t--Q) 0 9 ~-uer "<t I 3: 0 I s: ,... + 0 I 9~-oaa ~ ('I) -0 , ~ ~ + g~-AON C\1 0 ~ 9~-PO + ..... 0 I s: g~-das + 9~-onv 0 0 0 0 0 0 0 (!) 10 "<t C') C\1 ..... 0 ci ci ci ci ci ci ci 9~-flnv 9~-1nr co ..- ~ 9~-unr t -~ ...... 0 ..- I c. 9~-keV\1 3: -t -·cs CJ) r:: CD -..- 9~-Jd\f I 0 3: r:: t 0 += ~ -LO r:: 9 ~ -JBV\1 ..- Q) I () 3: r:: + 0 0 C\1 9 ~-qa.:J "<t ('I') ~ ~ .r:: + 1--CIO ,... 9 ~-uer == (") ..- ~ 0 + ,... ~ s~-~aa C\1 -..- 0 ~ ~ + g~-AON ..-~ 9~-PO + 0 ..- I 3: s~-das + s~-6nv 0 0 0 0 0 0 0 <0 ll) "<t (Y) C\1 ...... 0 0 0 0 0 0 0 0 BHV-1 BHV-2 BHV-3 Date Ra-226 U-Nat Pb-210 Th-232 Ra-226 U-Nat Pb-210 Th-232 Ra-226 U-Nat Pb-210 Th-232 9/7/1980 0.65 0.42 --0.34 0.42 --0.42 0.42 - 9/8/1981 0.4 1.8 --0.3 0.6 --0.3 0.6 -- 12/3/1981 0.79 0.77 --0.44 0.56 --0.89 0.42 -- 6/30/1982 0.423 0.384 --0.412 0.18 --0.265 0.207 -- 5/5/1983 0.471 0.41 . -0.569 0.55 --0.461 0.34 . - 6/4/1984 0.713 0.866 --0.618 0.683 --0.489 0.471 -- 10112/1984 2.96 0.886 --2.33 0.069 -. 2.88 0.721 - - 8/28/1985 1.63 0.8 -. 2.19 0.424 --2.27 0.424 -- 8/111986 0.369 0.654 -. 0.466 0.866 . -0.382 0.694 . - 8117/1987 0.6 0.8 -. 1.5 0.9 . . 0.8 0.6 -- 8/28/1988 1.5 1.6 --1.3 0.7 -. 0.6 0.9 . - 8/25/1988 1.2 1.6 --1.1 3 -. 0.8 1 -- 8/111990 2.9 5.8 . -1 1.4 --0.8 1.4 - 8/5/1991 3.9 8.8 . . 1.7 2.6 -. 2.6 5.7 -- 8/13/1992 1.2 2.2 --0.9 1.4 --0.8 1.2 -- 8/13/1993 2 1.7 --1.4 1.7 --1.1 1.9 -. 8/3/1994 1 1.6 -0.7 0.8 . -0.7 0.9 -. 8/28/1995 2.81 4.7 -. 0.68 0.2 . . 0.88 0.65 . - 8113/1996 1.7 2.15 --0.6 0.46 . -0.3 0.21 -- 8/1/1997 0.54 0.31 --0.56 0.16 -. 0.41 0.27 . - 711/1998 1.6 3.05 -. 0.7 0.58 -. 0.5 0.45 . . 8/24/1999 2.27 1.74 -. 0.78 0.84 --0.53 0.42 . 12/1/2000 1.51 1.21 --0.81 0.53 . -* * -. 8/23/2001 1 I --0.6 0.3 . -0.4 0.3 -- 8/1/2002 1.3 1.35 -. 0.9 0.524 . . 0.5 0.297 -- 8/5/2003 0.8 0.99 -. 0.6 0.79 --0.5 0.33 . - 8/9/2004 0.6 0.61 -. 0.4 0.25 -. 0.4 0.22 . - 8/3/2005 0.9 0.96 --0.7 0.34 --0.6 0.27 -- 8/7/2006 0.7 0.76 --0.44 0.25 -. 0.41 0.25 -- 8/8/2007 1.1 2.37 -. 0.7 0.53 -. 0.2 0.55 . . 8/20/2008 0.9 1.23 . . 0.3 0.43 -. 0.6 0.98 -- 8/10/2009 0.8 0.88 . . 0.7 0.54 --0.7 1.08 -- 8/2/2010 1.3 1.09 -. 1 1.49 --0.8 0.62 . - 8/23/2011 0.9 1.32 -. 0.4 0.32 --0.4 0.4 - 8/20/2012 0.5 1.96 --0.4 0.54 --0.7 1.09 -- 8/2112013 0.7 1.013 . . 0.3 0.405 -. 0.6 1.35 . - 8/25/2014 0.8 0.945 -0.4 0.54 . . 0.5 0.675 . - 8/18/2015 0.9 1.215 1.2 0.2 0.6 0.608 0.8 0.3 0.3 0.338 0.7 0.3 8/9/2016 0.5 0.4725 0.4 0.2 0.4 0.27 0.2 0.4 0.5 0.54 0.9 0.2 -Data not available. Table 1-1 WHITE MESA MILL Soil Sampling Results at BHV Stations 1-8 lP' rg ( Ci/ ) BHV-4 BHV-5 Ra-226 U-Nat Pb-210 Th-232 Ra-226 U-Nat Pb-210 0.41 12.194 --0.23 14.89 - 0.2 3 -0.3 0.6 - 0.75 0.63 --0.55 0.42 - 0.478 0.26 --0.449 0.216 - 0.643 0.34 . -0.147 0.14 . 0.124 0.324 . -0.132 0.31 . 3.49 0.804 . . 2.55 0.817 - 4.33 0.294 . -1.28 0.577 - 0.396 0.826 --0.728 0.836 - 1.2 0.7 . -1.5 1.3 . I 1.3 . -3.8 5 - 1.1 1.4 . -2.9 5.7 . 1.8 1.3 --3.7 3.2 - 1.8 2.6 . -2.5 4.4 - 0.9 0.9 --1.1 1.8 . 0.8 1.6 . . 4.8 3.5 - 0.7 1.1 --3 3.8 - 0.58 0.24 . -2.8 1.6 . 0.5 0.52 . -1.9 2.01 . 0.41 0.26 . . 1.7 1.5 - I 1.19 . -3 2.76 - 0.84 0.77 . . 3.27 3.15 - 0.83 1.22 --2.81 3.25 - 0.9 I --1.2 1.1 - 1.2 1.49 . -2.4 2.81 . 0.6 0.43 -0.28 0.42 . 0.6 0.51 --I 1.4 - 0.6 0.38 --0.7 0.41 . 0.52 0.48 --1.4 1.3 - 0.5 0.74 -. 1.1 1.45 . 0.5 0.79 . . 0.8 1.33 - 0.8 0.61 --2.6 2.98 - 1.3 1.69 . 1.7 1.69 - 0.5 0.58 . . I 1.48 - 0.6 0.81 . . 1.6 2.7 - 0.3 0.54 . -1.1 1.62 - 0.7 0.743 . . 2.8 3.71 - 0.5 0.54 0.2 0.3 1.2 1.215 1.0 0.5 0.2025 0.09 0.4 1.2 0.54 0.4 BHV-6 BHV-7 BHV-8 Th-232 Ra-226 U-Nat Pb-210 Th-232 Ra-226: U-Nat Pb-210 Tb-232 Ra-226 U-N at Pb-210 Tb-232 ---- --- ------- ------- ----. -. -. ----- -. -. -. . -. . . --. --. ---. ---. -. ---. --- . --. --- ---. -. . --. --•. -----. - -. . . --- . . . . . -- -. . -. -- ---. --- -. --. -- . --- --. . --. . -. . . ---. ----. -. -. -- - . . --. --. -0.6 0.53 . . --- -0.9 1.4 ----. - -I 1.2 -. . --- . 0.78 0.65 --. . . . . 0.8 0.93 --. --- -0.5 0.67 -. -. -. -0.5 0.81 ---. -. . 0.8 0.87 . ---. - -0.6 0.86 . -. --. . 0.8 1.37 . . . . -. . 0.5 0.743 . -. --- . 0.4 0.81 ------ 0.3 0.4 1.418 0.3 0.3 0.7 1.755 0.5 0.09 1.0 0.338 0.8 0.05 0.4 0.8 0.8775 0.3 0.2 0.8 0.54 0.2 0.5 0.5 0.135 0.08 0.3 ~..:.011 ' ~0~ N-Ull • umph~ date Ra-226 U-Nat Pb-210 Th-232 Ra-226 U-N at Pb-210 Tit-232 Ra-226 U-Nat Pb-210 Aug-15 0.30 0.47 0.80 0.30 0.50 0.41 0.30 0.30 0.60 0.61 0.90 Aug-16 0.50 0.20 0.60 0.20 0.60 0.20 0.40 0.50 0.50 0.20 0.60 Table 1-2 WHITE MESA MILL Soil Sampling Results in the Four Cardinal Directions lP~ rg, ( Ci! ) _Jit-04 ~0'8 Th-232 L~u-226 U-Ntlt J>b-'2Jl!O 'fiJ-232 illa.,Pl6 U-.!!i;1t IJ?l;-~,Jll) 'iJl\-232 0.40 0.60 0.41 0.20 0.20 0.80 0.95 1.00 0.30 0.40 0.70 0.14 0.60 0.40 0.90 0.34 0.50 0.40 S..'Olt ~I)!> S-0,~ :n~-~6 (! -JN:ill llb-2Ut0 'ijb-232 \Ra-2~(' I·U·:N<l~ P,b-2ltO, 1'11"2-3ii IRu-226 t~-1'\f::dl "fAL-~11loJ !lllt4~~ 0.30 0.20 1.10 0.30 0.60 0.54 0.50 0.60 o.3o I 0.34 1.10 0.06 0.40 0.14 0.30 0.08 0.20 0.05 0.70 0.20 o.2o I o.o7 0.80 0.30 E-(11 E-02 E-03 Sample date l,{a-226 U-N!!t Pb-210 rt1J-232 Ra-2:26 U-Nat Pb-210 Th-232 Ra-226 0-Nat Pb-210 Th-232 Ra-226 Aug-15 2.60 3.11 2.40 0.20 1.30 1.69 1.00 0.20 1.20 2.70 0.70 0.30 0.90 Aug-16 1.40 0.61 0.50 0.30 1.70 0.47 0.40 0.20 1.60 0.61 0.30 0.30 1.30 Table 1-2 WHITE MESA MILL Soil Sampling Results in the Four Cardinal Directions lP1 rg. ( Ci/ ) E-04 E-(15 E-06 U-N at Pb-210 Th-232 Ra-226 U-Nat Pb-210 Th-232 Ra-226 0 -Nat Pb-210 1.69 0.70 0.20 4.90 9.11 3.70 0.20 2.60 3.11 2.10 0.74 0.40 0.20 4.00 2.16 0.30 0.30 4.00 2.90 0.40 Th-232 0.20 0.20 E-07 E-08 :E-09 Ra-226 U-Nat Pb-210 Th-232 Ra-226 U-Nat Pb-210 Th-232 Ra-226 U-N at Pb-210 Th-232 0.50 0.74 0.30 0.10 3.50 4.79 3.20 0.20 2.00 3.51 2.10 0.20 1.20 0.34 0.06 0.08 3.50 1.62 0.50 0.20 2.50 1.35 0.30 0.20 E-10 E-U E-12 Ra-226 U-Nat Pb-210 Th-232 Ra-226 0-Nat Pb-210 Th-23"2 Ra-226 U-Nat Pb-210 Th-232 Ra-226 1.80 3.51 2.80 0.40 1.30 2.09 1.60 0.10 0.60 0.74 0.60 0.20 0.60 2.00 1.08 0.40 0.30 0.80 0.41 0.20 0.20 0.50 0.07 0.50 0.30 1.00 Table 1-2 WHITE :MESA MILL Soil Sampling Results in the Four Cardinal Directions ,pi rg, ( Ci/ ) E-13 E-14 E-15 U-Nat Pb-210 Th-232 Ra-226 U-Nat Pb-210 Th-232 Ra-226 U-Nat Pb-210 0.41 0.70 0.20 0.40 0.54 1.10 0.20 0.40 0.47 1.10 0.07 0.20 0.10 0.40 0.07 0.08 0.20 0.40 O.Q7 1.10 Th•232 0.20 0.20 E-16 I! E-17 E-18 Ra-226 U-Nat Pb-21Q Th-232 Ra-226 U-"Nat Pb-210 Th-232 Ra-226 U-N"at }.>b-210 Th-232 0.50 0.34 0.80 0.30 0.50 0.41 1.30 0.30 0.60 0.34 0.90 0.30 0.40 0.20 0.70 0.30 0.30 O.Q7 0.70 0.20 0.30 0.14 0.40 0.20 Table I-2 WHITE MESA MILL Soil Sampling Results in the Four Cardinal Directions Table 1-2 WHITE MESA MILL Soil Sampling Results in the Four Cardinal Directions Table I-3 WHITE MESA MILL Soil Sampling Results Duplicate Sample Results (pCi/g) Duplicate RPD results are outside of the 35% RPD limit. EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 February 03, 2017 Energy Fuels Resources (USA) Inc 225 Union Blvd Ste 600 Lakewood, CO 80228-1826 Work Order: C16080582 Project Name: Annual Soils 2016 ANALYTICAL SUMMARY REPORT Energy Laboratories, Inc. Casper WY received the following 56 samples for Energy Fuels Resources (USA) Inc on 8/12/2016 for analysis. LabiD Client Sample ID Collect Date Receive Date Matrix Test c 16080582-001 N01 08/09/16 8:26 08/12/16 Soil Metals by ICP/ICPMS, Total Percent Moisture Digestion For RadioChemistry Lead 210 Radium 226 Thorium, Isotopic c 16080582-002 N02 08/09/16 8:52 08/12/16 Soil Same As Above c 16080582-003 N03 08/09/16 8:54 08/12/16 Soil Same As Above c 16080582-004 N04 08/09/16 9:01 08/12/16 Soil Same As Above c 16080582-005 N05 08/09/16 9:02 08/12/16 Soil Same As Above c 16080582-006 E01 08/09/16 9:08 08/12/16 Soil Same As Above c 16080582-007 E02 08/09/16 9:12 08/12/16 Soil Same As Above c 16080582-008 E03 08/09/16 9:16 08/12/16 Soil Same As Above c 16080582-009 E04 08/09/16 9:18 08/12/16 Soil Same As Above c 16080582-01 0 E05 08/09/16 9:23 08/12/16 Soil Same As Above C16080582-011 E06 08/09/16 9:27 08/12/16 Soil Same As Above c 16080582-012 E07 08/09/16 9:30 08/12/16 Soil Same As Above c 16080582-013 E08 08/09/16 9:51 08/12/16 Soil Same As Above c 16080582-014 E09 08/09/16 9:56 08/12/16 Soil Same As Above c 16080582-015 E10 08/09/16 9:59 08/12/16 Soil Same As Above c 16080582-016 E11 08/09/16 10:02 08/12/16 Soil Same As Above c 16080582-017 E12 08/09/16 10:08 08/12/16 Soil Same As Above c 16080582-0 18 E13 08/09/16 10:20 08/12/16 Soil Same As Above c 16080582-019 E14 08/09/16 10:26 08/12/16 Soil Same As Above c 16080582-020 E15 08/09/1610:28 08/12/16 Soil Same As Above c 16080582-021 E16 08/09/1610:33 08/12/16 Soil Same As Above c 16080582-022 E17 08/09/16 1 0:39 08/12/16 Soil Same As Above c 16080582-023 E18 08/09/16 1 0:44 08/12/16 Soil Same As Above c 16080582-024 S01 08/09/16 10:51 08/12/16 Soil Same As Above Page 1 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.&90.2218 • Gillette, WY 8&&.&8&.7175 • Helena, MT 817.472.0711 ANALYTICAL SUMMARY REPORT c 16080582-025 S02 08/09/16 8:30 08/12/16 Soil Same As Above c 16080582-026 S03 08/09/16 12:47 08/12/16 Soil Same As Above c 16080582-027 W01 08/09/16 8:31 08/12/16 Soil Same As Above c 16080582-028 W02 08/09/16 8:38 08/12/16 Soil Same As Above c 16080582-029 W03 08/09/16 8:43 08/12116 Soil Same As Above c 16080582-030 W04 08/09/16 8:46 08/12/16 Soil Same As Above C16080582-031 W05 08/09/1613:51 08/12/16 Soil Same As Above c 16080582-032 W06 08/09/1613:47 08/12/16 Soil Same As Above c 16080582-033 W07 08/09/1612:44 08/12/16 Soil Same As Above c 16080582-034 W08 08/09/16 13:40 08/12/16 Soil Same As Above c 16080582-035 W09 08/09116 13:36 08/12/16 Soil Same As Above c 16080582-036 W10 08/09/1613:33 08/12/16 Soil Same As Above c 16080582-037 W11 08/09/16 13:13 08/12/16 Soil Same As Above c 16080582-038 W12 08/09/16 13:16 08/12/16 Soil Same As Above c 16080582-039 W13 08/09/16 13:22 08/12/16 Soil Same As Above c 16080582-040 W14 08/09/16 13:26 08/12/16 Soil Same As Above c 16080582-041 W15 08/09/16 12:57 08/12/16 Soil Same As Above c 16080582-042 W16 08/09/16 12:33 08/12/16 Soil Same As Above c 16080582-043 W17 08/09/1612:37 08/12/16 Soil Same As Above c 16080582-044 W18 08/09/16 12:42 08/12/16 Soil Same As Above c 16080582-045 BHV-1 08/09/16 9:04 08/12/16 Soil Same As Above c 16080582-046 BHV-2 08/09/16 9:42 08/12/16 Soil Same As Above c 16080582-04 7 BHV-3 08/09/16 9:23 08/12/16 Soil Same As Above C16080582-048 BHV-4 08/09/1610:12 08/12/16 Soil Same As Above c 16080582-049 BHV-5 08/09/16 9:54 08/12/16 Soil Same As Above c 16080582-050 BHV-6 08/09/1610:05 08/12/16 Soil Same As Above c 16080582-051 BHV-7 08/09/16 9:21 08/12/16 Soil Same As Above c 16080582-052 BHV-8 08/09/16 8:58 08/12/16 Soil Same As Above c 16080582-053 WestWater 08/09/16 9:00 08/12/16 Soil Same As Above c 16080582-054 E65 08/09/16 10:02 08/12/16 Soil Same As Above c 16080582-055 W70 08/09/1613:51 08/12/16 Soil Same As Above c 16080582-056 S75 08/09/16 8:30 08/12/16 Soil Same As Above The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QNQC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Page 2 of 70 EN::RGY Report Approved By: Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 8&6.886.7175 • Helena, MT 877.472.0711 ANALYTICAL SUMMARY REPORT Digitally signed by Corinne Wagner Date: 2017.02.03 08:58:22 -07:00 Page 3 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 871.472.0711 CLIENT: Project: Work Order: Energy Fuels Resources (USA) Inc Annual Soils 2016 C16080582 REVISED/SUPPLEMENTAL REPORT Revised Date: 02/03/17 Report Date: 1 0/26/16 CASE NARRATIVE The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on 1/31/2017 for the addition of Th232 that was requested on the chain of custody. Sample(s) were initially logged and reported as Th230. The data presented here is from that recheck/additional analysis. The report has been revised and replaces any previously issued report in its entirety. BRANCH LABORATORY SUBCONTRACT ANALYSIS Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4°C (±2°C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h-Energy Laboratories, Inc. -Helena, MT eli-cs -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; Oregon: WY200001 , Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin . Please verify Ell's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com . Page 4 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 08:26 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-001 Client Sample ID: N01 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.3 mg/kg-dry 0.6 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.05 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15/16 10:28/ smm 0.03 SW6020 08/31/16 21:341 sf E909.0 09128116 11 :44 I eli-cs E909.0 09128116 11 :44 I eli-cs E909.0 09128116 11 :44 I eli-cs E903.0 09114116 07:441 dmf E903.0 09114116 07:441 dmf E903.0 09114116 07:441 dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL -Maximum contaminant level. ND-Not detected at the reporting limit. D-RL increased due to sample matrix. Page 5 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 08:52 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-002 Client Sample ID: N02 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.3 mglkg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.6 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.5 pCilg-dry 0.09 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:281 smm 0.03 SW6020 08131116 21:361 sf E909.0 09128116 13:27 I eli-cs E909.0 09128116 13:27 I eli-cs E909.0 09128116 13:27 I eli-cs E903.0 09114116 07:441 dmf E903.0 09114116 07:441 dmf E903.0 09114116 07 :441 dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D-RL increased due to sample matrix. Page 6 of 70 EN:RGY Trust our People. Trust our Data. www.energyl~b.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 08:54 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-003 Client Sample ID: N03 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units NO wt% 0.3 mglkg-dry 0.6 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.4 pCilg-dry 0.07 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15/16 10:281 smm 0.03 SW6020 08131116 21:391 sf E909.0 09128116 06:351 eli-cs E909.0 09128116 06:351 eli-cs E909.0 09128116 06:351 eli-cs E903.0 09114116 07:44 I dmf E903.0 09114116 07:44 I dmf E903.0 09114116 07:441 dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 7 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:01 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-004 Client Sample ID: N04 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADION UC Ll DES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.6 wt% 0.2 mglkg-dry 0.6 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.7 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.4 pCilg-dry 0.07 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:29 I smm 0.03 SW6020 08131116 21:41 I sf E909.0 09128116 15:10 I eli-cs E909.0 09128116 15:10 I eli-cs E909.0 09128116 15:10 I eli-cs E903.0 09114116 07:44 I dmf E903.0 09114116 07:44 I dmf E903.0 09114116 07:44 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 8 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:02 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-005 Client Sample ID: NOS Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.6 wt% 0.5 mglkg-dry 0.5 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.9 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.4 pCilg-dry 0.07 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:291 smm 0.03 SW6020 08131116 21:441 sf E909.0 09128116 16:531 eli-cs E909.0 09128116 16:531 eli-cs E909.0 09128116 16:531 eli-cs E903.0 09114116 07:441 dmf E903.0 09114116 07:44 I dmf E903.0 09114116 07:441 dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 9 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com ---_____ _, Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.890.2218 • Gillette, WY 868.688.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:08 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 LabiD: c 16080582-006 Client Sample ID: E01 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units 1.0 wt% 0.9 mglkg-dry 0.5 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 1.4 pCilg-dry 0.3 pCi!g-dry 0.04 pCilg-dry 0.3 pCilg-dry 0.06 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115/16 10:291 smm 0.03 SW6020 08131116 21:46 I sf E909.0 09128116 18:361 eli-cs E909.0 09128116 18:361 eli-cs E909.0 09128116 18:361 eli-cs E903.0 09114116 07:441 dmf E903.0 09114116 07:441 dmf E903.0 09114116 07:441 dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 10 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Collage Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena , MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03117 Report Date: 1 0/26/16 Collection Date: 08/09/16 09:12 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: C16080582-007 Client Sample ID: E02 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.4 wt% 0.7 mglkg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 1.7 pCilg-dry 0.3 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:291 smm 0.03 SW6020 08131116 21 :58 I sf E909.0 09128116 20:19 I eli-cs E909.0 09128116 20:19 I eli-cs E909.0 09128116 20:19 I eli-cs E903.0 09114116 07:441 dmf E903.0 09114116 07:441 dmf E903.0 09114116 07:441 dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D-RL increased due to sample matrix. Page 11 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:16 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-008 Client Sample ID: E03 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.8 wt% 0.9 mglkg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 1.6 pCilg-dry 0.3 pCilg-dry 0.04 pCilg-dry 0.3 pCilg-dry 0.06 pCilg-dry 0.1 pCilg-dry MDC-Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 02 D2974 08/15116 10:30 I smm 0.03 SW6020 08/31116 22:01 I sf E909.0 09/28116 22:02/ eli-cs E909.0 09128116 22:02/ eli-cs E909.0 09/28116 22:02/ eli-cs E903.0 09/14/16 07:44/ dmf E903.0 09/14/16 07:44/ dmf E903.0 09/14/16 07:44/ dmf E908.0 09/14116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 12 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena. MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 09:18 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: lab ID: Annual Soils 2016 c 16080582-009 Client Sample ID: E04 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.9 wt% 1.1 mglkg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 1.3 pCilg-dry 0.3 pCi/g-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.04 pCi/g-dry 0.1 pCi/g-dry MDC-Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:30 I smm 0.03 SW6020 08131116 22:03 I sf E909.0 09128116 23:46 I eli-cs E909.0 09128116 23:46 I eli-cs E909.0 09128116 23:46 I eli-cs E903.0 09114116 07:44 I dmf E903.0 09/14116 07:44 I dmf E903.0 09114116 07:44 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 13 of 70 I EI\ERGY . ' Trust our People. Trust our Data. www.energylab.lOm Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.888.7175 • Helena, MT 877.472.0711 LABORATORY ANAL YTJCAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 09:23 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-010 Client Sample ID: E05 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.3 wt% 3.2 mglkg-dry 0.3 pCilg-dry 0.1 pCilg-dry 0.2 pCilg-dry 4.0 pCilg-dry 0.8 pCilg-dry 0.04 pCilg-dry 0.3 pCilg-dry 0.05 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers 0 MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:30 I smm 0.03 SW6020 08131116 22:06 I sf E909.0 09129116 01:29 I eli-cs E909.0 09129116 01 :29 I eli-cs E909.0 09129116 01 :29 I eli-cs E903.0 09114116 07:44 I dmf E903.0 09114116 07:44 I dmf E903.0 09114116 07:44 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. 0-RL increased due to sample matrix. Page 14 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.688.7175 • Helena, MT 877.412.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:27 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: C16080582-011 Client Sample ID: E06 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units NO wt% 4.3 mg/kg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 4.0 pCilg-dry 0.8 pCi/g-dry 0.04 pCi/g-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15/16 10:41/ smm 0.03 SW6020 08/31116 22:08/ sf E909.0 09/29/16 03:12 I eli-cs E909.0 09129116 03:12 I eli-cs E909.0 09129116 03:12 I eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 15 of70 EI\ERGY -.-Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 868.688.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 09:30 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-012 Client Sample ID: EO? Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.5 mg/kg-dry 0.06 pCi/g-dry 0.1 pCi/g-dry 0.2 pCi/g-dry 1.2 pCi/g-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.08 pCilg-dry 0.02 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:411 smm 0.03 SW6020 0813111622:111sf E909.0 09129116 04:55 I eli-cs E909.0 09/29116 04:551 eli-cs E909.0 09129116 04:55 I eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 16 of 70 EI\ERGY Trust our People. Trust our Data. www.energyiJb.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 868.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03117 Report Date: 1 0/26/16 Collection Date: 08/09/16 09:51 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: C16080582-013 Client Sample ID: E08 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radi~m 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.3 wt% 2.4 mg/kg-dry 0.5 pCi/g-dry 0.2 pCilg-dry 0.2 pCilg-dry 3.5 pCilg-dry 0.7 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15116 10:42 I smm 0.03 SW6020 08131116 22:13 I sf E909.0 09129116 06:38 I eli-cs E909.0 09129116 06:38 I eli-cs E909.0 09129116 06:38/ eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:571 eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 17 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 09:56 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: C16080582-014 Client Sample ID: E09 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units 0.4 wt% 2.0 mg/kg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 2.5 pCilg-dry 0.5 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15116 10:42 I smm 0.03 SW6020 08131/16 22:16/ sf E909.0 09129116 08:21 I eli-cs E909.0 09129116 08:21 I eli-cs E909.0 09129116 08:21 I eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 18 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 886.688.7175 • Helena, MT 871.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 09:59 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-015 Client Sample ID: E10 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.7 wt% 1.6 mglkg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 2.0 pCilg-dry 0.4 pCilg-dry 0.04 pCilg-dry 0.3 pCilg-dry 0.06 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:42 I smm 0.03 SW6020 08131116 22:18 I sf E909.0 09129116 10:04 I eli-cs E909.0 09129116 10:04 I eli-cs E909.0 09129116 10:04 I eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO-Not detected at the reporting limit. D-RL increased due to sample matrix. Page 19 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 10:02 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-016 Client Sample ID: E11 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.4 wl% 0.6 mglkg-dry 0.2 pCilg-dry 0.1 pCilg-dry 0.2 pCilg-dry 0.8 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.05 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:42 I smm 0.03 SW6020 08131116 22:31 I sf E909.0 09129116 11 :4 7 I eli-cs E909.0 09129116 11 :4 7 I eli-cs E909.0 09129116 11 :4 7 I eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 20 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 1 0:08 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-017 Client Sample ID: E12 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.5 wt% 0.1 mglkg-dry 0.5 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.3 pCilg-dry 0.06 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 10:431 smm 0.03 SW6020 08131116 22:331 sf E909.0 09129116 13:30 I eli-cs E909.0 09129116 13:30 I eli-cs E909.0 09129116 13:30 I eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 21 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 10:20 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-018 Client Sample ID: E13 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units 1.3 wt% 0.1 mg/kg-dry 0.2 pCilg-dry 0.1 pCilg-dry 0.2 pCilg-dry 1.0 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.1 pCilg-dry 0.02 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:431 smm 0.03 SW6020 08131116 22:36 I sf E909.0 09129116 15:13 I eli-cs E909.0 09129116 15:131 eli-cs E909.0 09129116 15:13 I eli-cs E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E903.0 09114116 09:40 I dmf E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 22 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 1 0:26 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-019 Client Sample ID: E14 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units ND wt% 0.1 mglkg-dry 0.08 pCilg-dry 0.1 pCilg-dry 0.2 pCilg-dry 0.4 pCilg-dry 0.09 pCilg-dry 0.05 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15/16 10:43/ smm 0.03 SW6020 08131116 22:381 sf E909.0 09129116 16:57 I eli-cs E909.0 09129116 16:57 I eli-cs E909.0 09129116 16:57 I eli-cs E903.0 10124116 08:20 I Irs E903.0 10124116 08:20 I Irs E903.0 1 0124116 08:20 I Irs E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 23 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Collage Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 10:28 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-020 Client Sample ID: E15 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.1 mglkg-dry 1.1 pCilg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.4 pCilg-dry 0.1 pCilg-dry 0.05 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15116 10:43 I smm O.Q3 SW6020 0813111622:411sf E909.0 09129116 18:40 I eli-cs E909.0 09129116 18:40 I eli-cs E909.0 09129/16 18:40 I eli-cs E903.0 10124116 08:20 I trs E903.0 10124116 08:20 I trs E903.0 10124116 08:20 I trs E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng E908.0 09114116 09:57 I eng MCL -Maximum contaminant level. ND-Not detected at the reporting limit. D-RL increased due to sample matrix. Page 24 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 o Casper, WY 888.235.0515 College Station, TX 888.690.2218 o Gillette, WY 866.686.7175 o Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 10:33 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-021 Client Sample ID: E16 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units NO wt% 0.3 mglkg-dry 0.7 pCi/g-dry 0.3 pCi/g-dry 0.2 pCilg-dry 0.4 pCi/g-dry 0.08 pCi/g-dry 0.03 pCilg-dry 0.3 pCi/g-dry 0.06 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15/16 10:441 smm 0.03 SW6020 09102/16 15:42 I sf E909.0 09130/16 06:41 I eli-cs E909.0 09/30/16 06:41 I eli-cs E909.0 09/30116 06:41 I eli-cs E903.0 09/19/16 10:00 I dmf E903.0 09119/16 10:00 I dmf E903.0 09/19/16 10:00 I dmf E908.0 09114/16 14:45 I eng E908.0 09114116 14:451 eng E908.0 09114116 14:45 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 25 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 10:39 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 LabiD: c 16080582-022 Client Sample ID: E17 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL -Quality control limit. Result Units ND wt% 0.1 mglkg-dry 0.7 pCilg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.3 pCilg-dry 0.08 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15/16 10:44 I smm 0.03 SW6020 09102116 15:44 I sf E909.0 09130116 08:24 I eli-cs E909.0 09130116 08:24 I eli-cs E909.0 09130116 08:241 eli-cs E903.0 09119/16 10:00 I dmf E903.0 09119/16 10:00 I dmf E903.0 09119/16 10:00 I dmf E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 26 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 10:44 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: C16080582-023 Client Sample ID: E18 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.2 wt% 0.2 mglkg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.3 pCilg-dry 0.08 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry MDC-Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15116 10:441 smm 0.03 SW6020 0910211616:071sf E909.0 09130116 01:311 eli-cs E909.0 09130116 01:311 eli-cs E909.0 09130116 01 :31 I eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 27 of70 EI\ERGY Trust our People. Trust our Data. www.energyl a b.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.&90.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 10:51 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-024 Client Sample ID: S01 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units NO wt% 0.2 mglkg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.4 pCilg-dry 0.09 pCilg-dry 0.04 pCilg-dry 0.08 pCilg-dry 0.02 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 10:44 I smm 0.03 SW6020 09102116 16:09 I sf E909.0 09130116 10:07 I eli-cs E909.0 09130116 10:07 I eli-cs E909.0 09130116 10:07 I eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 28 of70 EN:RGY ; Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7115 • Helena, MT 817.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 08:30 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-025 Client Sample ID: S02 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result Units NO wt% 0.08 mglkg-dry 0.7 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.06 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15116 10:441 smm 0.03 SW6020 09102116 16:121 sf E909.0 09130116 11 :50 I eli-cs E909.0 09130116 11 :50 I eli-cs E909.0 09130116 11 :50 I eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:451 eng E908.0 09114116 14:45 I eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 29 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 12:47 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-026 Client Sample ID: S03 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.1 mglkg-dry 0.8 pCilg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.05 pCilg-dry 0.04 pCilg-dry 0.3 pCilg-dry 0.05 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15116 11:00 I smm 0.03 SW6020 09102116 16:14 I sf E909.0 09130116 13:33 I eli-cs E909.0 09130116 13:33 I eli-cs E909.0 09130116 13:33 I eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 30 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 08:31 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-027 Client Sample ID: W01 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.5 wt% 0.3 mglkg-dry 0.6 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.6 pCIIg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.5 pCIIg-dry 0.09 pCilg-dry 0.1 pCIIg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:01 I smm 0.03 SW6020 09102116 16:171 sf E909.0 09130116 15:161 eli-cs E909.0 09130116 15:16 I eli-cs E909.0 09130116 15:161 eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 31 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03117 Report Date: 1 0/26/16 Collection Date: 08/09/16 08:38 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-028 Client Sample ID: W02 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.3 mglkg-dry 0.8 pCi/g-dry 0.3 pCi/g-dry 0.2 pCilg-dry pCilg-dry 0.2 pCi/g-dry 0.04 pCi/g-dry 0.3 pCilg-dry 0.06 pCi/g-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15/16 11:011 smm 0.03 SW6020 09/02/16 16:19/ sf E909.0 09130/16 16:59/ eli-cs E909.0 09130/16 16:59/ eli-cs E909.0 09130116 16:591 eli-cs E903.0 09/19/16 10:00 I dmf E903.0 09/19/16 10:00 I dmf E903.0 09/19/16 10:00 I dmf E908.0 09/14116 14:451 eng E908.0 09/14116 14:451 eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 32 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 08:43 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-029 Client Sample ID: W03 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.4 mglkg-dry 1.1 pCilg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.8 pCilg-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.1 pCilg-dry MDC-Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:01 I smm 0.03 SW6020 09102116 16:22 I sf E909.0 09130116 18:42 I eli-cs E909.0 09130116 18:42 I eli-cs E909.0 09130116 18:42 I eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D-RL increased due to sample matrix. Page 33 of 70 EI\ERGY •' Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 08:46 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-030 Client Sample ID: W04 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.8 wt% 0.4 mglkg-dry 2.0 pCilg-dry 0.6 pCilg-dry 0.2 pCilg-dry 0.6 pCilg-dry 0.1 pCilg-dry 0.04 pCIIg-dry 0.2 pCIIg-dry 0.05 pCIIg-dry 0.2 pCilg-dry MDC-Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 11 :02 I smm 0.03 SW6020 09102116 16:24 I sf E909.0 09130116 20:26 I eli-cs E909.0 09130116 20:26 I eli-cs E909.0 09130116 20:26 I eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 34 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Colleg& Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 13:51 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-031 Client Sample ID: W05 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 2.0 wt% 0.3 mglkg-dry 2.5 pCilg-dry 0.8 pCilg-dry 0.2 pCilg-dry 0.4 pCilg-dry 0.09 pCilg-dry 0.03 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 11:02 I smm 0.03 SW6020 09102116 16:27 I sf E909.0 09130116 22:09 I eli-cs E909.0 09130116 22:091 eli-cs E909.0 09130116 22:091 eli-cs E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E903.0 09119116 10:00 I dmf E908.0 09114116 14:451 eng E908.0 09114116 14:45 I eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 35 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 13:47 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-032 Client Sample ID: W06 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.4 wt% 0.1 mglkg-dry 0.8 pCilg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.4 pCilg-dry 0.09 pCilg-dry 0.03 pCilg-dry 0.1 pCilg-dry 0.03 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 11:02 I smm 0.03 SW6020 09102116 16:39 I sf E909.0 09130116 23:52 I eli-cs E909.0 09130116 23:52 I eli-cs E909.0 09130116 23:52 I eli-cs E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng MCL-Maximum contaminant level. NO-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 36 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 12:44 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-033 Client Sample ID: W07 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.1 mglkg-dry 1.6 pCilg-dry 0.5 pCilg-dry 0.2 pCilg-dry 0.3 pCi/g-dry 0.07 pCIIg-dry 0.04 pCilg-dry 0.3 pCilg-dry 0.07 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:031 smm 0.03 SW6020 09102116 16:42 I sf E909.0 10101116 01:351 eli-cs E909.0 10101116 01:351 eli-cs E909.0 10101116 01:351 eli-cs E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E903.0 09119116 12:081 dmf E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 37 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03117 Report Date: 1 0/26/16 Collection Date: 08/09/16 13:40 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-034 Client Sample ID: W08 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADION UC Ll DES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units NO wt% 0.2 mglkg-dry 1.5 pCilg-dry 0.5 pCilg-dry 0.2 pCilg-dry 0.4 pCilg-dry 0.09 pCi/g-dry 0.03 pCi/g-dry 0.2 pCI/g-dry 0.04 pCi/g-dry 0.1 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 11:031 smm 0.03 SW6020 09102116 16:44 I sf E909.0 10101116 03:181 eli-cs E909.0 10101116 03:181 eli-cs E909.0 1 0101116 03:18 I eli-cs E903.0 09119/16 12:08/ dmf E903.0 09119/16 12:081 dmf E903.0 09/19116 12:081 dmf E908.0 09/14/16 14:45/ eng E908.0 09/14/16 14:45/ eng E908.0 09/14116 14:45/ eng MCL-Maximum contaminant level. NO-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 38 of 70 EI\ERGY Trust our People. Trust our Data. 1'1 ww.ene rgyl a b.corn Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette. WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANAL YTJCAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 13:36 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-035 Client Sample ID: W09 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units NO wt% 0.07 mglkg-dry 1.2 pCilg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.06 pCilg-dry 0.03 pCilg-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 11:031 smm 0.03 SW6020 09102116 16:47 I sf E909.0 10101116 05:01 I eli-cs E909.0 10101116 05:01 I eli-cs E909.0 10101116 05:01 I eli-cs E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E908.0 09114116 14:45 I eng E908.0 09114116 14:451 eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 39 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 13:33 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-036 Client Sample ID: W10 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.8 wt% 0.1 mglkg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.4 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.4 pCilg-dry 0.08 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15/16 11 :03 I smm 0.03 SW6020 09102116 16:49 I sf E909.0 10101116 06:44 I eli-cs E909.0 10101116 06:44 I eli-cs E909.0 10101116 06:44 I eli-cs E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 40 of?O EI\ERGY •' Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7115 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 13:13 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-03 7 Client Sample ID: W11 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADION UC L1 DES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.2 mg/kg-dry 0.3 pCilg-dry 0.2 pCi/g-dry 0.2 pCilg-dry 0.3 pCilg-dry 0.07 pCilg-dry 0.03 pCi/g-dry 0.2 pCi/g-dry 0.03 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15/16 11:04/ smm 0.03 SW6020 09/02/16 16:52 I sf E909.0 10/01116 08:27 I eli-cs E909.0 10/01116 08:27 I eli-cs E909.0 10101116 08:27 I eli-cs E903.0 09119116 12:08 I dmf E903.0 09/19116 12:08 I dmf E903.0 09119116 12:08/ dmf E908.0 09114116 14:45/ eng E908.0 09114116 14:45/ eng E908.0 09114116 14:451 eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 41 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 888.686.7175 • Helena. MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 13:16 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-038 Client Sample ID: W12 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.9 wt% 0.08 mglkg-dry 0.7 pCilg-dry 0.3 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.06 pCilg-dry 0.03 pCilg-dry 0.09 pCilg-dry 0.02 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 11:041 smm 0.03 SW6020 09102116 16:54 I sf E909.0 10101116 10:10 I eli-cs E909.0 10101116 10:10 I eli-cs E909.0 10101116 10:10 I eli-cs E903.0 09119116 12:081 dmf E903.0 09119116 12:081 dmf E903.0 09119116 12:081 dmf E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng E908.0 09114116 14:45 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 42 of70 EI\ERGY Trust our People. Trust our Data. www.e nergyla b.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 13:22 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-039 Client Sample ID: W13 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC ------- Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.2 mg/kg-dry 0.5 pCi/g-dry 0.2 pCi/g-dry 0.2 pCi/g-dry 0.3 pCi/g-dry 0.07 pCi/g-dry 0.03 pCi/g-dry 0.1 pCi/g-dry 0.02 pCi/g-dry 0.2 pCi/g-dry MDC-Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:04 I smm 0.03 SW6020 09102116 16:571 sf E909.0 10101/16 11:53/ eli-cs E909.0 10/01/16 11:531 eli-cs E909.0 10101116 11:53/ eli-cs E903.0 09119116 12:08 I dmf E903.0 09/19116 12:08 I dmf E903.0 09119116 12:08 I dmf E908.0 09114116 14:45/ eng E908.0 09114/16 14:45/ eng E908.0 09/14/16 14:45/ eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D-RL increased due to sample matrix. Page 43 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.&86.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 13:26 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-040 Client Sample ID: W14 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.4 mglkg-dry 0.4 pCilg-dry 0.2 pCilg-dry 0.2 pCilg-dry 0.002 pCilg-dry 0.02 pCilg-dry 0.03 pCilg-dry 0.4 pCilg-dry 0.07 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 0811511611:041smm 0.03 SW6020 09102116 16:59 I sf E909.0 1 0101116 13:36 I eli-cs E909.0 10101116 13:36 I eli-cs E909.0 10101116 13:36 I eli-cs E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E903.0 09119116 12:08 I dmf E908.0 09114116 14:46 I eng E908.0 09114116 14:46 I eng E908.0 09114116 14:46 I eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D-RL increased due to sample matrix. Page 44 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 12:57 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 LabiD: c 16080582-041 Client Sample ID: W15 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADION UC Ll DES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result Units ND wt% 0.4 mglkg-dry 0.3 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.2 pCilg-dry 0.06 pCilg-dry 0.03 pCilg-dry -30 pCilg-dry 2610 pCilg-dry 0 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11 :05 I smm 0.03 SW6020 09102116 21:141 sf E909.0 10102116 00:531 eli-cs E909.0 10102116 00:53 I eli-cs E909.0 10102116 00:531 eli-cs E903.0 09119116 12:04 I dmf E903.0 09119116 12:041 dmf E903.0 09119116 12:04 I dmf E908.0 09116116 09:361 eng E908.0 09116116 09:36 I eng E908.0 09116116 09:36 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 45 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 12:33 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-042 Client Sample ID: W16 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADION UC Ll DES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.4 wt% 0.6 mglkg-dry 0.3 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.3 pCilg-dry 0.08 pCilg-dry 0.03 pCilg-dry -0.05 pCilg-dry 4.4 pCilg-dry 0 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 11 :06 I smm 0.03 SW6020 09102116 21:17 I sf E909.0 10102116 02:36 I eli-cs E909.0 10102116 02:36 I eli-cs E909.0 10102116 02:361 eli-cs E903.0 09119116 12:05 I dmf E903.0 09119116 12:051 dmf E903.0 09119116 12:051 dmf E908.0 09116116 09:361 eng E908.0 09116116 09:36 I eng E908.0 09116116 09:36 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 46 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 12:37 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-043 Client Sample ID: W17 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.6 wt% 0.5 mglkg-dry 0.6 pCilg-dry 0.2 pCilg-dry 0.1 pCilg-dry 0.4 pCilg-dry 0.09 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15116 11:06 I smm 0.03 SW6020 09102116 21 :29 I sf E909.0 10101116 20:14 I eli-cs E909.0 10101116 20:141 eli-cs E909.0 10101116 20:141 eli-cs E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E908.0 09116116 09:36 I eng E908.0 09116116 09:36 I eng E908.0 09116116 09:36 I eng MCL-Maximum contaminant level. NO-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 47 of 70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.412.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 12:42 DateReceived: 08112/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-044 Client Sample ID: W18 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units NO wt% 0.5 mglkg-dry 0.8 pCilg-dry 0.2 pCilg-dry 0.1 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.03 pCilg-dry 0.5 pCilg-dry 0.09 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 11:11 I smm 0.03 SW6020 09102116 21 :32 I sf E909.0 10102116 04:19 I eli-cs E909.0 10102116 04:19 I eli-cs E909.0 10102116 04:19 I eli-cs E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E908.0 09116116 09:361 eng E908.0 09116116 09:361 eng E908.0 09116116 09:361 eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 48 of70 EI\ERGY " ' Trust our People. Trust our Data. www.e ne rgyla b.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:04 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-045 Client Sample ID: BHV-1 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.2 wt% 0.7 mglkg-dry 0.4 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0_2 02974 08115116 11:121 smm O.Q3 SW6020 09102116 21 :44 I sf E909.0 10102116 06:02 I eli-cs E909.0 10102116 06:02 I eli-cs E909.0 10102116 06:02 I eli-cs E903.0 09119116 12:051 dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:051 dmf E908.0 09116116 09:36/ eng E908.0 09/16116 09:361 eng E908.0 09116116 09:36/ eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 49 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LAB ORA TORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 09:42 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-046 Client Sample ID: BHV-2 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.3 wt% 0.4 mglkg-dry 0.2 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.4 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.4 pCilg-dry 0.07 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 0811511611:12 I smm 0.03 SW6020 09102116 21 :47 I sf E909.0 10102116 07:45 I eli-cs E909.0 10102116 07:45 I eli-cs E909.0 10102116 07:45 I eli-cs E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E908.0 09116116 09:36 I eng E908.0 09116116 09:36 I eng E908.0 09116116 09:36 I eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D-RL increased due to sample matrix. Page 50 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.890.2218 • Gillette, WY 886.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:23 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-04 7 Client Sample ID: BHV-3 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.8 mglkg-dry 0.9 pCilg-dry 0.3 pCilg-dry 0.1 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.2 pCIIg-dry 0.04 pCIIg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:121 smm 0.03 SW6020 09102116 21 :49 I sf E909.0 10102116 09:28 I eli-cs E909.0 10102116 09:28 I eli-cs E909.0 10102116 09:28 I eli-cs E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:051 dmf E908.0 09116116 09:361 eng E908.0 09116116 09:361 eng E908.0 09116116 09:361 eng MCL-Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 51 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 10:12 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-048 Client Sample ID: BHV-4 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 2.1 wt% 0.3 mglkg-dry 0.09 pCilg-dry 0.09 pCilg-dry 0.1 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.4 pCilg-dry 0.07 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 02974 08115116 11:121 smm 0.03 SW6020 09102116 21 :52 I sf E909.0 10102116 11:11 I eli-cs E909.0 10102116 11:11 I eli-cs E909.0 10102116 11:111 eli-cs E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E908.0 09116116 09:361 eng E908.0 09116116 09:361 eng E908.0 09116116 09:36 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 52 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:54 Date Received: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-049 Client Sample ID: BHV-5 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units 2.1 wt% 0.8 mg/kg-dry 0.4 pCi/g-dry 0.2 pCilg-dry 0.1 pCilg-dry 1.2 pCilg-dry 0.2 pCilg-dry 0.04 pCilg-dry 0.4 pCilg-dry 0.08 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 0811511611 :131smm 0.03 SW6020 09102116 21 :54 I sf E909.0 10102116 12:54 I eli-cs E909.0 10102116 12:54 I eli-cs E909.0 10102116 12:54 I eli-cs E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E903.0 09119116 12:05 I dmf E908.0 09116116 09:36 I eng E908.0 09116116 09:36 I eng E908.0 09116116 09:36 I eng MCL-Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 53 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 10:05 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-050 Client Sample ID: BHV-6 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADION UC Ll DES Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 0.7 wt% 1.3 mg/kg-dry 0.3 pCi/g-dry 0.1 pCi/g-dry 0.1 pCi/g-dry 0.8 pCi/g-dry 0.2 pCi/g-dry 0.04 pCi/g-dry 0.2 pCi/g-dry 0.04 pCi/g-dry 0.2 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 02974 08/15/16 11:13/ smm 0.03 SW6020 09/02/16 21 :59/ sf E909.0 10/02/16 14:37 I eli-cs E909.0 10/02/16 14:37 I eli-cs E909.0 10/02/16 14:37 I eli-cs E903.0 09/19/16 12:05 I dmf E903.0 09/19/16 12:05 I dmf E903.0 09/19/16 12:05 I dmf E908.0 09/16/16 09:36/ eng E908.0 09/16/16 09:36/ eng E908.0 09/16/16 09:36/ eng MCL-Maximum contaminant level. NO-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 54 of 70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:21 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: C16080582-051 Client Sample ID: BHV-7 Analyses PHYSICAL CHARACTERISTICS Moisture METALS -TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result Units 1.1 wt% 0.8 mglkg-dry 0.2 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.8 pCilg-dry 0.2 pCilg-dry 0.03 pCilg-dry 0.5 pCilg-dry 0.09 pCilg-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15/16 11:13 I smm 0.03 SW6020 09/02116 22:02 1 sf E909.0 10102116 16:20 I eli-cs E909.0 10102116 16:20 I eli-cs E909.0 10102116 16:20 I eli-cs E903.0 09119116 12:05 I dmf E903.0 09119116 12:051 dmf E903.0 09119116 12:051 dmf E908.0 09/16116 09:36 I eng E908.0 09116116 09:361 eng E908.0 09116116 09:36 I eng MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 55 of70 EI\ERGY Trust our People. Trust our Data. www.ene rgyla b.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 08:58 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-052 Client Sample ID: BHV-8 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 1.0 wt% 0.2 mglkg-dry 0.08 pCilg-dry 0.09 pCilg-dry 0.1 pCilg-dry 0.5 pCilg-dry 0.1 pCilg-dry 0.03 pCilg-dry 0.3 pCilg-dry 0.06 pCilg-dry 0.1 pCilg-dry MDC-Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 08115116 11:131 smm 0.03 SW6020 09102116 22:04 I sf E909.0 10102116 18:031 eli-cs E909.0 10102116 18:03 I eli-cs E909.0 10102116 18:03 I eli-cs E903.0 09119116 14:191 dmf E903.0 09119116 14:19 I dmf E903.0 09119116 14:191 dmf E908.0 09116116 09:361 eng E908.0 09116116 09:361 eng E908.0 09116116 09:361 eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 56 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.corn Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Collage Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 09:00 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-053 Client Sample ID: WestWater Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.1 mglkg-dry 0.05 pCilg-dry 0.09 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.04 pCilg-dry 0.04 pCilg-dry 0.05 pCilg-dry 0.01 pCilg-dry 0.1 pCilg-dry MDC-Minimum detectable concentration Qualifiers D u u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 02974 0811511611 :141smm 0.03 SW6020 09102116 22:17 I sf E909.0 10102116 19:46 I eli-cs E909.0 10102116 19:46 I eli-cs E909.0 10102116 19:46 I eli-cs E903.0 09119/1614:191 dmf E903.0 09119116 14:191 dmf E903.0 09119116 14:191 dmf E908.0 09116116 09:36 I eng E908.0 09116116 09:361 eng E908.0 09116116 09:36 I eng MCL-Maximum contaminant level. NO-Not detected at the reporting limit. D-RL increased due to sample matrix. Page 57 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 871.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 1 0/26/16 Collection Date: 08/09/16 10:02 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-054 Client Sample ID: E65 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL -Anaiyte reporting limit. QCL-Quality control limit. Result Units 1.0 wt% 0.4 mglkg-dry 0.2 pCilg-dry 0.1 pCilg-dry 0.1 pCilg-dry 0.7 pCilg-dry 0.1 pCilg-dry 0.03 pCilg-dry 0.1 pCilg-dry 0.02 pCilg-dry 0.1 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 0811511611:141smm 0.03 SW6020 09/02116 22:19 I sf E909.0 10102116 21 :29 I eii-cs E909.0 10102116 21:29 I eli-cs E909.0 10/02116 21:29 I eli-cs E903.0 09119116 14:19 I dmf E903.0 09119116 14:19 I dmf E903.0 09119116 14:19 I dmf E908.0 09116116 09:36 I eng E908.0 09116116 09:36 I eng E908.0 09116116 09:36 I eng MCL -Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 58 of70 EN:RGY Trust our People. Trust our Data. www.energylab.corn Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7115 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 13:51 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-055 Client Sample ID: W70 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units 3.4 wt% 0.2 mg/kg-dry 0.3 pCi/g-dry 0.1 pCi/g-dry 0.1 pCilg-dry 0.6 pCilg-dry 0.1 pCi/g-dry 0.03 pCilg-dry 0.4 pCi/g-dry 0.08 pCi/g-dry 0.1 pCi/g-dry MDC -Minimum detectable concentration Qualifiers D MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15/16 11:151 smm 0.03 SW6020 09102116 22:22 I sf E909.0 10102/16 23:12/ eli-cs E909.0 10102/16 23:12 I eli-cs E909.0 10102116 23:121 eli-cs E903.0 09119116 14:19 I dmf E903.0 09119116 14:19/ dmf E903.0 09/19/16 14:191 dmf E908.0 09116116 09:36 I eng E908.0 09/16116 09:36 I eng E908.0 09116/16 09:36/ eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 59 of70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Collection Date: 08/09/16 08:30 DateReceived: 08/12/16 Matrix: Soil Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Lab ID: c 16080582-056 Client Sample ID: S75 Analyses PHYSICAL CHARACTERISTICS Moisture METALS-TOTAL Uranium RADIONUCLIDES Lead 210 Lead 210 precision(±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 232 Thorium 232 precision (±) Thorium 232 MDC Report Definitions: RL-Analyte reporting limit. QCL-Quality control limit. Result Units ND wt% 0.09 mg/kg-dry 0.1 pCi/g-dry 0.1 pCi/g-dry 0.1 pCi/g-dry 0.3 pCilg-dry 0.06 pCilg-dry 0.04 pCilg-dry 0.2 pCi/g-dry 0.04 pCi/g-dry 0.2 pCilg-dry MDC -Minimum detectable concentration Qualifiers D u U -Not detected at minimum detectable concentration MCU RL QCL Method Analysis Date I By 0.2 D2974 08/15/16 11:15/ smm 0.03 SW6020 09102/16 22:24 I sf E909.0 10/03/16 00:55 I eli-cs E909.0 10/03/16 00:55 I eli-cs E909.0 10/03116 00:55/ eli-cs E903.0 09/19116 14:19/ dmf E903.0 09/19116 14:19/ dmf E903.0 09/19116 14:19/ dmf E908.0 09116116 09:36/ eng E908.0 09116/16 09:36/ eng E908.0 09116/16 09:361 eng MCL-Maximum contaminant level. ND -Not detected at the reporting limit. D-RL increased due to sample matrix. Page 60 of?O EN:RGY Trust our People. Trust our Data. www.e nergylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.&90.2218 • Gillette, WY 8&&.&86.7175 • Helena, MT 871.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Revised Date: 02/03/17 Client: Energy Fuels Resources (USA) Inc Report Date: 10/26/16 Project: Annual Soils 2016 Work Order: C16080582 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: E903.0 Batch: 48176 Lab ID: LCS1-48176 Laboratory Control Sample Run :G5000VV_160908B 09/14/16 07:44 Radium 226 1.5 pCi/g-dry 95 80 120 LabiD: MB-48176 3 Method Blank Run:G5000VV_160908B 09/14/16 07:44 Radium 226 0.01 pCi/g-dry Radium 226 precision (±) 0.007 pCi/g-dry Radium 226 MDC 0.009 pCi/g-dry LabiD: C16080582-001 AM 51 Sample Matrix Spike Run:G5000VV_160908B 09/14/16 07:44 Radium 226 1.8 pCi/g-dry 84 70 130 Lab ID: C16080582-001AMS1 Sample Matrix Spike Duplicate Run: G5000VV_160908B 09/14/16 07:44 Radium 226 1.6 pCi/g-dry 73 70 130 10.0 49.8 Method: E903.0 Batch: 48199 LabiD: LCS1-48199 Laboratory Control Sample Run: G5000VV_160909A 09/19/16 10:00 Radium 226 1.4 pCi/g-dry 93 80 120 Lab ID: MB-48199 3 Method Blank Run: G5000VV_160909A 09/19/16 10:00 Radium 226 0.005 pCi/g-dry u Radium 226 precision (±) 0.005 pCi/g-dry Radium 226 MDC 0.008 pCi/g-dry Lab ID: C16080582-021AMS1 Sample Matrix Spike Run:G5000VV_1 60909A 09/19/16 10:00 Radium 226 1.7 pCi/g-dry 84 70 130 LabiD: C16080582-021AMS1 Sample Matrix Spike Duplicate Run: G5000VV_160909A 09/19/16 10:00 Radium 226 1.6 pCi/g-dry 77 70 130 6.7 49.7 Method: E903.0 Batch: 48176 Lab ID: LCS1-48176 Laboratory Control Sample Run: G5000VV_161014B 10/24/16 08:20 Radium 226 0.3 pCi/g-dry 102 80 120 Lab ID: MB-48176 3 Method Blank Run: G5000VV_161014B 1 0/24/16 08:20 Radium 226 0.007 pCi/g-dry u Radium 226 precision (±) 0.006 pCi/g-dry Radium 226 MDC 0.009 pCi/g-dry Lab ID: C16080582-001 AMS 1 Sample Matrix Spike Run: G5000VV_161014B 10/24/16 08:20 Radium 226 1.7 pCi/g-dry 79 70 130 Lab ID: C16080582-001 AMS1 Sample Matrix Spike Duplicate Run: G5000VV_161014B 10/24/16 08:20 Radium 226 1.7 pCi/g-dry 82 70 130 0.4 20 Qualifiers: RL-Ana lyle reporting limit. ND-Not detected at the reporting limit. MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration Page 61 of 70 EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Work Order: C16080582 Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Analyte Count Result Units Method: E903.0 Lab ID: LCS1-48230 Radium 226 Lab ID: MB-48230 Radium 226 Radium 226 precision (±) Radium 226 MDC Lab ID: C16080582-041 AMS 1 Radium 226 Lab ID: C16080582-041AMS1 Radium 226 Qualifiers: RL-Analyte reporting limit. 3 MDC -Minimum detectable concentration Laboratory Control Sample 1.4 pCi/g-dry Method Blank 0.006 pCi/g-dry 0.005 pCi/g-dry 0.008 pCi/g-dry Sample Matrix Spike 1.6 pCi/g-dry Sample Matrix Spike Duplicate 1. 7 pCi/g-dry RL %REC Low Limit High Limit Run: G542M_160909A 91 80 120 Run:G542M_160909A Run: G542M_160909A 85 70 130 Run:G542M_160909A 94 70 130 NO -Not detected at the reporting limit. RPD RPDLimit Qual 8.7 Batch: 48230 09/19/16 12:04 09/19/16 12:04 u 09/19/16 12:05 09/19/16 12:05 49.6 U -Not detected at minimum detectable concentration Page 62 of 70 ' EI\ERGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette. WY 866.686.7175 • Helena, MT 877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Work Order: C16080582 Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Analyte Method: E908.0 LabiO: LCSS-48176 Thorium 230 Lab 10: C16080582-005AMS5 Thorium 230 LabiO: C16080582-005AMS5 Thorium 230 Lab 10: MB-48176 Thorium 230 Thorium 230 MDC Thorium 232 precision (±) Method: E908.0 Lab 10: C16080582-024AMS5 Thorium 230 Lab 10: C16080582-024AMS5 Thorium 230 Count Result Units Laboratory Control Sample 2.3 pCi/g-dry Sample Matrix Spike 3.6 pCi/g-dry Sample Matrix Spike Duplicate 3.5 pCi/g-dry 3 Method Blank 0.002 pCi/g-dry 0.01 pCi/g-dry 0.006 pCi/g-dry Sample Matrix Spike 2.5 pCi/g-dry Sample Matrix Spike Duplicate 2.0 pCi/g-dry RL %REC Low Limit High Limit RPO Run: EGG-ORTEC_160907B 90 80 120 Run: EGG-ORTEC_160907B 118 70 130 Run: EGG-ORTEC_160907B 114 70 130 2.8 Run: EGG-ORTEC_160907B Run: EGG-ORTEC_160909A 90 70 130 Run: EGG-ORTEC_160909A 69 70 130 24 RPOLimit Qual Batch: 48176 09/14/16 09:57 09/14/16 09:57 09/14/16 09:57 48 09/14/16 09:57 u Batch: 48199 09/14/16 14:45 09/14/16 14:45 48.1 s -Spike response is outside of the acceptance range for this analysis. Since the LCS and the RPD recoveries are acceptable, the response is considered to be matrix related The batch is approved. Lab 10: MB-48199 Thorium 230 Thorium 230 MDC Thorium 232 precision (±) LabiO: LCSS-48199 Thorium 230 Method: E908.0 Lab 10: LCSS-48230 Thorium 230 3 Method Blank 0.003 pCi/g-dry 0.01 pCi/g-dry 0.006 pCi/g-dry Laboratory Control Sample 5.3 pCi/g-dry Laboratory Control Sample 6.4 pCi/g-dry Run: EGG-ORTEC_160909A Run: EGG-ORTEC_160909A 106 80 120 Run: EGG-ORTEC_160912A 128 80 120 -LCS response is outside of the acceptance range for this analysis. Since the MB, MS, and MSD are acceptable the batch is approved. LabiO: C16080582-044AMS5 Thorium 230 Lab 10: C16080582-044AMS5 Thorium 230 LabiO: MB-48230 Thorium 230 Thorium 230 MDC Thorium 232 precision (±) Qualifiers: RL -Analyte reporting limit. Sample Matrix Spike 4.1 pCi/g-dry Sample Matrix Spike Duplicate 5.0 pCi/g-dry 3 Method Blank 0.006 pCi/g-dry 0.02 pCi/g-dry 0.008 pCi/g-dry MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration Run: EGG-ORTEC_160912A 77 70 130 Run: EGG-ORTEC_160912A 95 70 130 20 Run: EGG-ORTEC_160912A ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. 09/14/16 14:46 u 09/14/16 14:46 Batch: 48230 09/16/16 09:36 s 09/16/16 09:36 09/16/16 09:36 48 09/16/16 09:36 u Page 63 of70 EI\ERGY . · Trust our People. Trust our Data . www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 86&.&8&.7175 • Helena, MT 877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Revised Date: 02/03/17 Client: Energy Fuels Resources (USA) Inc Report Date: 10/26/16 Project: Annual Soils 2016 Work Order: C16080582 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: E909.0 Batch: T _25516 LabiD: MB-25516 3 Method Blank Run: SUB-T69878 09/28/16 03:08 Lead 210 0.09 pCi/g-dry u Lead 210 precision(±) 0.1 pCi/g-dry Lead 210 MDC 0.2 pCi/g-dry Lab ID: LCS3-25516 Laboratory Control Sample Run: SUB-T69878 09/28/16 04:52 Lead 210 2.2 pCi/g-dry 89 80 120 Lab ID: C16080582-003A Sample Matrix Spike Run: SUB-T69878 09/28/16 08:18 Lead 210 2.6 pCi/g-dry 84 70 130 Lab ID: C16080582-003A Sample Matrix Spike Duplicate Run: SUB-T69878 09/28/16 10:01 Lead 210 2.7 pCi/g-dry 89 70 130 4.0 71 .1 Method: E909.0 Batch: T_25517 Lab ID: MB-25517 3 Method Blank Run: SUB-T69893 09/29/16 22:05 Lead 210 0.09 pCi/g-dry u Lead 210 precision (±) 0.1 pCi/g-dry Lead 210 MDC 0.2 pCi/g-dry LabiD: LCS3-25517 Laboratory Control Sample Run: SUB-T69893 09/29/16 23:48 Lead 210 1.4 pCi/g-dry 53 80 120 s -LCS response is outside of the acceptance range for this analysis. Since the MB, MS. and MSO are acceptable the batch is approved. Lab 10: C16080582-023A Sample Matrix Spike Run: SUB-T69893 09/30/16 03:15 Lead 210 2.8 pCi/g-dry 103 70 130 Lab ID: C16080582-023A Sample Matrix Spike Duplicate Run: SUB-T69893 09/30/16 04:58 Lead 210 2.4 pCi/g-dry 87 70 130 15 71 .8 Method: E909.0 Batch: T_25550 Lab ID: MB-48230 3 Method Blank Run: SUB-T69894 10/01/16 16:48 Lead 210 0.02 pCi/g-dry u Lead 210 precision(±) 0.09 pCi/g-dry Lead 210 MDC 0.1 pCi/g-dry Lab ID: LCS3-48230 Laboratory Control Sample Run: SUB-T69894 10/01/16 18:31 Lead 210 2.2 pCi/g-dry 90 80 120 Lab ID: C16080582-043A Sample Matrix Spike Run: SUB-T69894 10/01/16 21:57 Lead 210 3.4 pCi/g-dry 120 70 130 Lab ID: C16080582-043A Sample Matrix Spike Duplicate Run: SUB-T69894 10/01/16 23:27 Lead 210 3.6 pCi/g-dry 127 70 130 3.8 69.8 Qualifiers: RL -Analyte reporting limit. ND-Not detected at the reporting limit. MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits. U -Not detected at minimum detectable concentration Page 64 of70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 86&.&8&.7175 • Helena, MT 877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Revised Date: 02/03/17 Report Date: 10/26/16 Work Order: C16080582 Project: Annual Soils 2016 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW6020 LabiO: ICV Uranium LabiO: ICSA Uranium Lab 10: ICSAB Uranium Method: SW6020 Lab 10: MB-48176 Uranium LabiO: LCS2-48176 Uranium Lab 10: C16080582-020AMS2 Uranium Lab 10: C16080582-020AMSO Uranium Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Initial Calibration Verification Standard 0.0482 mg/L 0.00030 Interference Check Sample A 0.000182 mg/L 0.00030 Interference Check Sample AB 1.20E-05 mg/L 0.00030 Method Blank 0.007 mg/kg 0.0008 Laboratory Control Sample 0.47 mg/kg 0.010 Sample Matrix Spike 2.0 mg/kg-dry 0.026 Sample Matrix Spike Duplicate 1.4 mg/kg-dry 0.026 96 93 94 61 Analytical Run: ICPMS2-C_160831A 08/31/16 16:01 90 110 Run: ICPMS2-C_160831A Run: ICPMS2-C_160831A 75 125 Run: ICPMS2-C_160831A 75 125 Run : ICPMS2-C_160831A 75 125 08/31/16 16:04 08/31/16 16:06 Batch: 48176 08/31/16 21 :26 08/31/16 21 :29 08/31/16 22:46 08/31/16 22:48 s ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 65 of 70 EN:RGY Trust our People. Trust our Data. www.energylab.com Billings, MT 800.735.4489 • Casper, WY 888.235.0515 College Station, TX 888.690.2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 QAIQC Summary Report Prepared by Casper, WY Branch Revised Date: 02/03/17 Report Date: 10/26/16 Work Order: C 16080582 Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2016 Analyte Count Result Method: SW6020 Units RL %REC Low Limit High Limit RPD RPDLimit Qual Analytical Run: ICPMS2-C_160902A LabiD: ICV Initial Calibration Verification Standard 09/02/16 12:26 Uranium 0.0483 mg/L LabiD: ICSA Interference Check Sample A Uranium 0.000173 mg/L Lab ID: ICSAB Interference Check Sample AB Uranium 1.66E-05 mg/L Method: SW6020 Lab ID: MB-48199 Method Blank Uranium NO mg/kg LabiD: LCS2-48199 Laboratory Control Sample Uranium 1.1 mg/kg Lab ID: C16080582-022ADIL Serial Dilution Uranium NO mg/kg-dry Lab 10: C16080582-022AMS2 Sample Matrix Spike Uranium 1.2 mg/kg-dry Lab ID: C16080582-040ADIL Serial Dilution Uranium 0.26 mg/kg-dry Method: SW6020 LabiD: MB-48230 Method Blank Uranium 0.02 mg/kg Lab ID: LCS2-48230 Laboratory Control Sample Uranium 1.1 mg/kg Lab ID: C16080582-042ADIL Serial Dilution Uranium 1.9 mg/kg-dry Lab ID: C16080582-042AMS2 Sample Matrix Spike Uranium 1.4 mg/kg-dry Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits. 0.00030 97 90 110 0.00030 0.00030 Run: ICPMS2-C_160902A 0.0008 Run: ICPMS2-C_160902A 0.010 110 75 125 Run: ICPMS2-C_160902A 0.13 Run: ICPMS2-C_160902A 0.026 89 75 125 Run: ICPMS2-C_160902A 0.13 Run: ICPMS2-C_160902A 0.0008 Run: ICPMS2-C_160902A 0.010 110 75 125 Run: ICPMS2-C_160902A 0.13 Run: ICPMS2-C_160902A 0.026 67 75 125 NO -Not detected at the reporting limit. R -RPD exceeds advisory limit. 09/02/16 12:28 09/02/16 12:31 Batch: 48199 09/02/16 15:35 09/02/16 15:37 09/02/16 15:47 10 09/02/16 15:49 09/02/16 17:12 43 10 R Batch: 48230 09/02/16 20:57 09/02/16 20:59 09/02/16 21:19 110 10 R 09/02/16 21 :22 s Page 66 of70 EI\ERGY Trust our People. Trust our Data. www.energylab com Work Order Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Tessa Parke Reviewed by: Tessa Parke Reviewed Date: 8/12/2016 Shipping container/cooler in good condition? Custody seals intact on all shipping container(s)/cooler(s)? Custody seals intact on all sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH. DO, Res Cl, Sulfite, Ferrous Iron, etc.) Temp Blank received in all shipping container(s)/cooler(s)? Container/Temp Blank temperature: Water-VOA vials have zero heads pace? Water-pH acceptable upon receipt? Standard Reporting Procedures: Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes D oc Yes D Yes D Billings, MT 800.735.4489 • Casper, WY 888.235.0515 Gillette, WY 8&&.&86.7175 • Helena, MT 877.472.0711 C16080582 Date Received: 8/12/2016 Received by: dcj NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD Carrier name: Next Day Air Not Present D Not Present D Not Present 0 Not Applicable 0 NoVOA vials submitted 0 Not Applicable 0 Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Contact and Corrective Action Comments: None Page 67 of 70 ... ,..,.., Sheet 1 of 1 ,. ;'(·: . ,. CHAIN OF CUSTODY Samples Shipped to: Energy Laboraties Contact: Garrin Palmer --=2~39~3~sa--=l~t C~r-e-e~k ~H~wy-. -------Ph: 435 678 2221 Casper WY, 82601 gpalmer@energvtuels.com Chain of Custody/Sampling Analysis Request p . roject s amplers N a me Samplers Signature Annual Soils 2016 Garrin Palmer I 6~~ Time Sample ID Date Collected Collected Laboratory Analysis Requested N01 8/9/2016 826 Radium-226, Pb-210, Th-232, U-nat N02 8/9/2016 852 Aadium-226, Pb-210, Th-232, U-nat N03 8/9/2016 854 Radium-226, Pb-210, Th-232, U-nat N04 8/9/2016 901 Aadium-226, Pb-21 0, Th-232, U-nat NOS 8/9/2016 902 Radium-226, Pb-210, Th-232, U-nat E01 8/9/2016 908 Radium-226, Pb-21 0, Th-232, U-nat E02 8/9/2016 912 Radium-226, Pb-21 0, Th-232, U-nat E03 8/9/2016 916 Radium-226, Pb-210, Th-232, U-nat E04 8/9/2016 918 Radium-226, Pb-210, Th-232, U-nat E05 8/9/2016 923 Radium-226, Pb-21 0, Th-232, U-nat E06 8/9/2016 927 Aadium-226, Pb-21 0, Th-232, U-nat E07 8/9/2016 930 Radium-226, Pb-21 0, Th-232, U-nat E08 8/9/2016 951 Radium-226, Pb-21 0, Th-232, U-nat E09 8/9/2016 956 Radium-226, Pb-21 0, Th-232, U-nat E10 8/9/2016 959 Radium-226, Pb-21 0, Th-232, U-nat E11 8/9/2016 1002 Radium-226, Pb-21 0, Th-232, U-nat E12 8/9/2016 1008 Radium-226, Pb-210, Th-232, U-nat E13 8/9/2016 1020 Radium-226, Pb-21 0, Th-232, U-nat Comments: Please send report to Kathy Weinel at kweinel @energyfuels.com Relinquished By:(Sigb'~ Date/Time Received By:(Signature) Datemme G~ 8/10/2016 1230 Relinquished By: (Signature) Date/Time Received By:(Signature) gy;~ .......::;;;; h '{ ~ ""'- ~ -1/!ID .~ Sheet 1 of 1 ........ CHAIN OF CUSTODY Samples Shipped to: Energy Laboraties Contact: Garrin Palmer ~2~39~3~Sa~l~tC~re~e~k~H~wy--. --------------Ph:4356782221 Casper WY, 82601 gpalmer@enerqyfuels.com Chain of Custody/Sampling Analysis Request Project Samplers Name Samplers Signature Annual Soils 2016 Garrin Palmer I G-~-~~~ Time Sample 10 Date Collected Collected Laboratory Analysis Requested E14 8/9/2016 1026 Radium-226, Pb-21 0, Th-232, U-nat E15 8/9/2016 1028 Aadium-226, Pb-210, Th-232, U-nat E16 8/9/2016 1033 Radium-226, Pb-210, Th-232, U-nat E17 8/9/2016 1039 Radium-226, Pb-21 0, Th-232, U-nat E18 8/9/2016 1044 Radium-226, Pb-210, Th-232, U-nat S01 8/9/2016 1051 Radium-226, Pb-210, Th-232, U-nat S02 8/10/2016 830 Radium-226, Pb-210, Th-232, U-nat S03 8/9/2016 1247 Radium-226, Pb-210, Th-232, U-nat W01 8/9/2016 831 Radium-226, Pb-210, Th-232, U-nat W02 B/9/2016 838 Radium-226, Pb-21 0, Th-232, U-nat W03 B/9/2016 843 Radium-226, Pb-210, Th-232, U-nat W04 B/9/2016 846 Radium-226, Pb-21 0, Th-232, U-nat W05 8/9/2016 1351 Radium-226, Pb-21 0, Th-232, U-nat W06 B/9/2016 1347 Radium-226, Pb-21 0, Th-232, U-nat W07 8/9/2016 1244 Radium-226, Pb-21 0, Th-232, U-nat woe 8/9/2016 1340 Radium-226, Pb-21 0, Th-232, U-nat W09 8/9/2016 1336 Radium-226, Pb-21 0, Th-232, U-nat W10 8/9/2016 1333 Radium-226, Pb-210, Th-232, U-nat Comments: Please send report to Kathy Weinel at kweinel@energyf_uels.com Datemme Received By:(Signature) B/10/2016 1230 Date/Time Received By:(Signature) Date/Time Datemme -· ... : Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to; Energy Laboraties Contact: Garrin Palmer ~2~3~93~S~al~t~C~re~e~k~H~wy--.--------------Ph:4356782221 Casper WY, 82601 gpalmer@energvtuels.com Chain of Custody/Sampling Analysis Request Project s amplers N a me s amplers Signature Annual Soils 2016 Garrin Palmer I ~~~~ Time SampleiD Date Collected Collected Laboratory Analysis Requested E65 8/9/2016 1002 Radium-226, Pb-210, Th-232, U-nat W70 8/9/2016 1351 Radium-226, Pb-210, Th-232, U-nat S75 8110/2016 830 Radium-226, Pb-210, Th-232, U-nat Comments: Please send report to Kathy Weinel at kweinel@ energyfuels.com Relinquish"'! By,(SignalureQ~ Datemme Received By:(Signature) Date/Time ~-8/10/2016 1230 Relinquished By:(Signature) Date/Time Received By:(Signature) Date/Time ATTACHMENT J RADON MONITORING GRAPHS AND DATA LWc/9/~ 9 ~Oc/0~/0~ _J (.) w "0 9 ~Oc/9/L Q) -~ ::::l (.) (1j ~Oclvlv (.) .,- I > I WclvH co + 9Wc/Bc/6 9~0G/6G/9 "0 Q) N -(.) N (1j ,_ -N .D 9~0c/c/v ::::l I C/) s::: "0 0 c ::::l "'C 9~0c/LH 0 ,_ C) ca ~ (.) a: (1j co ,.... vwc/0816 .c. -:> ~ .,- :I: I v~Oc/Lc/9 > m I co v~Oclclv + 8 ~Oc/vc/c~ -"0 c 8 ~OcH/0 ~ ::::l e C) ~ (.) (1j ~Oc/~IL e C") I > I 8~0G/6G/8 co + 8 ~Oc/c/~ CX) ""' <D I!) '<t C") C\J ..-0 0 0 0 0 0 0 0 0 1\!::>d pCi\L 0 9 0 0 0 0 9 0 0 ~ 1\) (,.) ~ 01 0) -.....! to 1/2/201 + OJ 3/29/201 I < I (1.) -C'" 7/1/201 I» (") "' (Q ..... 0 c 10/1/201 .. :::J c.. ........ 12/24/201 + 4/2/201 OJ I < I m 1\) 6/27/201 :E :I: ;:::;: ::::r -;:: OJ 9/30/2014 I» 1\) (") "' (Q l:J ..... 0 c 1/7/201 . m :::J c.. c. U'J 0 c C'" 4/2/201 ::::J -..... I» I (") 1\) -(I) 1\) c.. 6/29/2015 1\) + 9/28/2015 OJ I 1/4/201 < I 1\) 0 I» (") c a (I) c.. m 7/5/201 0 r 10/10/201 1/5/2017 pCi\L 0 0 0 0 0 0 0 !=> 0 _. 1\) w ~ c.n 0> ""-~ (X) 1/2/2013 3/29/2013 7/1/2013 10/1/2013 12/24/2013 4/2/2014 6/27/2014 1 .I I I I I I I I tD + N :I: 9/30/2014 -;:: OJ w I < J] I 1/7/2015 w Q) a. 4/2/2015 1 Ill[' I I I I I I I I 0 ::l I N 6/29/2015 ~ N N 9/28/2015 1/4/2016 4/4/2016 7/5/2016 10/10/2016 1/5/2017 L~Oc/91~ 9 ~0?./0 ~10 ~ ....J () ~0?./9/L w "'0 Q) ..... as :::J ~0?./V/V 0 as () -.::t I 9~0?./V/~ > I Ill 9~0?./B"G/6 t N N 9 ~0?./6?./9 N "'0 I Q) ..... s::: 0 as 0 9~0?./c/v ..... ..... .0 "C :::J ca (f) "'0 a: 9~0?./LH c :::J 0 ~ ..... C) :> ~ 0 V~Oc/08/6 as ::I: CD ..c m ~ ~0?./L?./9 -.::t I > I Ill + 8Wc/vc/c~ ........ "'0 · ~OG/ ~/0 ~ c :::J e C) ~ 0 ~O?.H/L as .0 -C') I > 8W"G/6"G/8 I Ill 8 ~OG/G/~ + 00 I'-<0 I{) -.::t ('I') C\l T""" 0 0 0 0 0 0 0 0 0 1\!0d + OJ I < I VJ -0'" Dl 0 7\ (Q ..... 0 c ::J 0.. - + OJ I < I 01 :E ;:::;.: :J" OJ Dl 0 7\ (Q ..... 0 c ::J 0.. (f) c 0'" -..... Dl 0 -CD 0.. + OJ I < I 01 () Dl 0 c Dl -CD 0.. m () r 0 1/2/201 3/29/2013 7/1/201 9/30/2014 1/7/2015 4/2/2015 6/29/2015 9/28/2015 1/4/2016 4/4/2016 10/10/2016 1/5/2017 0 0 1\) :r.,.. 0 0> pCi\L 0 00 ...... ...... ...... 1\) :r.,.. ...... 0> OJ :I: -;:: CJ1 :a D) c. 0 ::J I 1\) 1\) 1\) L~OC::/9/~ 9~02:/0~/0~ ...J (.) w "'0 a> WC::/9/L ]i ::I (.) «i (.) 9~oc::tvtv <D I > :::r: Ill 9~octvl~ + 9~02:/82:/6 "'0 N a> 9WC::/6C::/9 t5 N ctl N ..... -..c I ::I c 9~oc::tc::tv en 0 "'C c:: "C ::I 0 ca ..... 9~02:/L/~ Cl a: ~ (.) ctl (0 co ..c:: ::> PWC::/0£/6 ~ :t: <D I m > :::r: Ill v~oc::tc::tv + £~02:/PC::/C::~ -"'C c:: ::I e ~OC::/~/0~ Cl ~ (.) ctl e ~OC::H/L C') I > :::r: Ill £~02:/62:/£ + £~02:/G/~ 0> co ,.... (0 10 """ C') C\J T""" 0 0 0 0 c) 0 0 0 0 0 1\!=>d ~OG/S/~ 9~0G/0~/0~ ...J () w "'0 Q) -n3 ~OG/S/L "3 (.) -ns () I'-I > N J: a:! N + N · ~OG/P/P I c:: 0 "'0 Q) "C 0 ~ ca -.0 a: :J 9~0G/P/~ U) "' "'0 c :> :J 0 .... J: Ol ~ (.) m n3 co WG/BG/6 ..c ~ I'-I > J: a:! S~OG/6G/9 + :0 c :J e Ol ~ (.) S~OG/G/P n3 .0 -(") I > J: a:! S~OG/L/~ + C\! CX) CD '<t C\J 0 ..... 0 0 0 0 1\!0d L~OG/9/~ ~OG/0~/0 ~ ...J () w "C Q) -~OG/9/L J2 :::::1 0 (ij () CX) I > ::I: N al + N WG/17/v N I c: "C 0 Q) -"'C 0 ~ ca -.0 a: 9~0G/t/~ :::::1 (/) CX) "C c > :::::1 e C) J: .::.:. 0 m ctl 1:0 9Wc/8c/6 ..c ~ co I > ::I: 1:0 9~0G/6G/9 + -"'0 c :::::1 e ~ 0 9~0G/G/t ctl .0 -('I) I > :I: 1:0 + 9~0G/L/~ CX) ....... co 1.0 '<t ('I) C\1 ,... 0 ci ci ci 0 ci 0 ci ci 1\!0d WhiteM ~ ----------------Mill Rad s .. -------0 ---------lin!! R Its* BHV-1 BHV-2 BHV-4 BHV-5 BHV-1 Calculated BHV-2 Calculated BHV-3 BHV-4 Calculated BHV-5 Calculated Date (pCi/L) ECL (pCi/L) ECL (pCi/L) (pCi/L) ECL (pCi/L) ECL 1/2/2013 0.1 0.71 0 0.34 0.6 0.4 0.5 0 1.43 3/29/2013 0.1 0.71 0 0.34 0.7 0.3 0.5 0.5 1.43 7/112013 0 0.71 0 0.34 0.06 0 0.5 0 1.43 10/112013 0.1 0.71 0 0.34 0.07 0 0.5 NA 1.43 12/24/2013 0.4 0.71 0 0.34 0.07 0.33 0.5 0.43 1.43 4/2/2014 0.2 0.71 0 0.34 0.06 0.04 0.5 0.54 1.43 6/27/2014 0.1 0.71 0 0.34 0.07 0 0.5 0.03 1.43 9/30/2014 0.2 0.71 0.1 0.34 0.1 0.2 0.5 0.3 1.43 117/2015 0.1 0.71 0 0.34 0.2 0.3 0.5 0.6 1.43 4/2/2015 0.23 0.71 0 0.34 0.07 0.23 0.5 0.43 1.43 6/29/2015 0.2 0.71 0.2 0.34 0.2 0.4 0.5 0.4 1.43 9/28/2015 0.2 0.71 0.1 0.34 0.3 0.2 0.5 0.6 1.43 114/2016 0.0 0.71 0.0 0.34 0.2 0.4 0.5 0.7 1.43 4/4/2016 0.0 0.71 0.1 0.34 0.2 0 0.5 0.7 1.43 7/5/2016 0.1 0.71 0.0 0.34 0.07 0 0.5 0.23 1.43 10/10/2016 0.06 0.71 0.0 0.34 0.35 0.30 0.5 0.38 1.43 115/2017 0.14 0.71 0.1 0.34 0.32 0.25 0.5 0.38 1.43 *-Measurements obtained from BHV-3 have been designated as background due to BHV-3's remoteness from the Mill site. The results in the table above are the above-background results with background (BHV-3) subtracted. Any negative values are reported as zero for graphical purposes. NA-Not Available-the canister was damaged. No data reported. NS-Not Sampled -EFRI installed and began radon sampling at BHV-7 and BHV-8 in the fourth quarter of 2014. BHV-6 BHV-6 Calculated (pCi/L) ECL 0.4 0.83 0.1 0.83 0 0.83 0 0.83 0.73 0.83 0.24 0.83 0.03 0.83 0.2 0.83 0.2 0.83 0.23 0.83 0.3 0.83 0.3 0.83 0.1 0.83 0.1 0.83 0 0.83 0.08 0.83 0.19 0.83 BHV-7 BHV-8 BHV-7 Calculated BHV-8 Calculated (pCi/L) ECL (pCi/L) ECL NS 1.12 NS 0.71 NS 1.12 NS 0.71 NS 1.12 NS 0.71 NS 1.12 NS 0.71 NS 1.12 NS 0.71 NS 1.12 NS 0.71 NS 1.12 NS 0.71 NS 1.12 NS 0.71 0.2 1.12 0.1 0.71 0.33 1.12 0.03 0.71 0.2 1.12 0.2 0.71 0 1.12 0.1 0.71 0.2 1.12 0.1 0.71 0 1.12 0 0.71 0 1.12 0 0.71 0.03 1.12 0 0.71 0 1.12 0.14 0.71 White Mesa Mill Radon Sampling Quartel"ly Field Blank Results Field Blank Date (pCi/L) 1/2/2013 2.4 3/29/2013 1.4 711/2013 0.7 10/1/2013 0.3 12/24/2013 0.7 4/2/2014 1.6 6/27/2014 1.1 9/30/2014 0.8 117/2015 1.4 4/2/2015 1.0 6/29/2015 1.7 9/28/2015 1.5 114/2016 1.8 4/4/2016 2.0 7/5/2016 1.1 10/10/2016 1.6 1/5/2017 1.6 Calculation of Location-Specific Effluent Concentration Limits for Radon Track Etch Monitoring Stations at White Mesa Mill Calculation Methodology For the purpose of evaluating alpha track data and compliance with the effluent concentration limit for radon, two referenced limits are listed in the regulations (1 0 CFR Part 20 Appendix B, Table 2, which are incorporated by reference into R313-15-302(2)(b)(i)). One limit (lx 10-10 uCi/ml or 0.1 pCi/1) is applicable in instances where radon daughters are present with the radon, and are in 100% equilibrium with the parent Rn-222. The other listed concentration limit (1 x 1 o-8 uCi/ml or 10 pCi/1) is applicable when radon daughters are not present. Both limits represent the concentration at which a member of the public would receive a 50 mrem dose assuming 100% (8760 hours) occupancy. At the White Mesa Mill, the assumption of 100% equilibrium of radon progeny with parent Rn- 222 is unrealistic given the short half-lives of the nuclides considered and the short travel time to the monitoring locations. Radon emanates from the ground (or mill tailings) without daughters present, and the daughters grow in over time. It is therefore necessary to evaluate radon daughter equilibrium at each air monitoring station utilizing site-specific wind speed and distance information to derive site-specific Effluent Concentration Limits (ECLs) for each station. Such disequilibrium situations and alternative calculations are anticipated by the regulations and, in particular, R313-15-302(3) provides a means by which the licensee may adjust the effluent concentration values in 10 CFR Part 20 Appendix B, Table 2, which are incorporated by reference into R313-15-302(2)(b)(i), to account for disequilibrium. The regulatory purpose of such an adjustment is to appropriately take into account the actual characteristics of the measured effluents, including radioactive decay equilibrium. An established (EPA, 1986) outdoor equilibrium formula to determine the appropriate Equilibrium Factor for use in calculating the ECL for disequilibrium conditions was used. The EPA expression of the outdoor Equilibrium Factor (EF) is derived by the following equation: EF = 1.0-0.0479exp<-rt4.39l-2.1963exp<-1138·6l + 1.2442exp<-r128.4l [Where: tis the travel time in minutes (distance/wind speed)] Once the Equilibrium Factor has been determined, the ECL for each air monitoring station is determined by dividing the 0.1 pCi/1 limit (for situations when daughters are present) by the Equilibrium Factor (EF). Results By utilizing the above formula, the appropriate (equilibrium adjusted) ECLs for the location was calculated. In developing the ECLs, distances and corresponding travel times have been determined by: • assuming a nominal centroid located approximately at the vanadium dryer stack, • calculating average wind speeds appropriate for each direction from the centroid to each monitoring station location, and • using Google Earth to develop the distances. Meteorological data collected at the Mill's Met Station were utilized to compute the average wind speed for different directions. These data are applicable and sufficient for the for the purpose of these calculations. It should be noted when comparing actual measurement values to the derived ECLs that the derived ECL provides ample protection for members of the public. More specifically, if dose calculations had been performed utilizing current ICRP 65 dose conversion conventions, the ECLs established here would represent approximately 25 mrem for continuous exposure at the monitoring stations. Therefore these values can serve as appropriate ALARA goals, since they yield doses well below the 100 mrem standard for individual members of the public. References United States Environmental Protection Agency (EPA). (1986). Final rule for radon-222 emissionsfrom licensed uranium mill tailings. Washington, D.C.: Office of Radiation Programs, U.S. Environmental Protection Agency. ATTACHMENT K CELL 2 RADON FLUX DATA Cell2 2016 Radon Flux Measurement Program White Mesa Mill 6425 South Highway 191 Blanding, Utah 84511 July 2016 Sampling Results Prepared for: Energy Fuels Resources (USA) Inc. 6425 S. Highway 191 P.O. Box 809 Blanding, Utah 84511 Prepared by: Tellco Environmental P.O. Box 3987 Grand Junction, Colorado 81502 TABLE OF CONTENTS Page I. INTRODUCTION ........................................................................................................................... I 2. SITE HISTORY AND DESCRIPTION .......................................................................................... I 3. REGULATORY REQUIREMENTS FOR THE SITE .................................................................... I 4. SAMPLING METHODOLOGY ...................................................................................................... I 5. FIELD OPERATIONS .................................................................................................................... 2 5.1 Equipment Preparation ....................................................................................................... 2 5.2 Sample Locations, Identification, and Placement.. ........................................................... 2 5.3 Sample Retrieval ............................................................................................................... 3 5.4 Environmental Conditions ................................................................................................ 3 6. SAMPLE ANALYSIS ..................................................................................................................... 4 6.1 Apparatus ........................................................................................................................... 4 6.2 Sample Inspection and Documentation ............................................................................. 4 6.3 Background and Sample Counting ..................................................................................... 4 7. QUALITY CONTROL (QC) AND DATA VALIDATION ........................................................... 5 7 .I Sensitivity .......................................................................................................................... 5 7.2 Precision ................................................................................................................. , ........... 5 7.3 Accuracy ............................................................................................................................ 5 7.4 Completeness ..................................................................................................................... 5 8. CALCULATIONS ........................................................................................................................... 6 9. RESULTS ........................................................................................................................................ 7 9.1 Mean Radon Flux ............................................................................................................... 7 9.2 Site Results ........................... , ............................................................................................. 8 References ....................................... t ••••••••••••••••••••••••••••••••••••••••••••••••••••••••• ; •••••••••••••••••••••• ~···~·····-·····•··· 9 Figure l ................................. _ ...... .., ................................................................................. i •••••••••••••••••••••••••• 10 Appendix A. Charcoal Canister Analyses Support Documents Appendix B. Recount Data Analyses Appendix C. Radon Flux Sample Laboratory Data, Including Blanks Appendix D. Sample Locations Map (Figure 2) i 1. INTRODUCTION During July 16-17, 2016 Tellco Environmental, LLC (Tellco) of Grand Junction, Colorado, provided support to Energy Fuels Resources (USA) Inc. (Energy Fuels) to conduct radon flux measurements on Cell 2 at its White Mesa Mill site. Pursuant to Utah Department of Environmental Quality (UDEQ) requirements, Energy Fuels conducts radon flux measurements on a semiannual basis. This report presents the radon flux measurements results for Cell 2 that represent the second half of the year 2016. Tellco was contracted to provide radon canisters, equipment, and canister-placement personnel as well as lab analysis of samples collected. Energy Fuels personnel provided support for loading and unloading charcoal from the canisters. This report details the procedures employed by Energy Fuels and Tellco to obtain the results presented in Section 9.0 of this report. 2. SITE DESCRIPTION The White Mesa Mill facility is located in San Juan County in southeastern Utah, six miles south of Blanding, Utah. The mill began operations in 1980 for the purpose of extracting uranium and vanadium from feed stocks. Cell 2, which has a total area of approximately 270,624 m2, has been filled and covered with interim cover. This cell is comprised of one region, an interim soil cover of varying thickness. There was no standing liquid and were no apparent exposed tailings within Cell 2 during this sampling. 3. REGULATORY REQUIREMENTS FOR CELL 2 Radon emissions from the uranium mill tailings at this site are regulated by the State of Utah's Division of Waste Management and Radiation Control (DWMRC). In accordance with DWMRC requirements specified in correspondence dated July 23, 2014, Energy Fuels must measure the radon flux on Cell2 in accordance with 40 CFR 61, Appendix B, Method 115, "Monitoring for Radon-222 Emissions" (2013) semiannually. The average annual measured radon flux for Cell2 shall not exceed a value of 20 picoCuries per meter squared per second (pCilm2 -s ). 4. SAMPLING METHODOLOGY Radon emissions were measured using Large Area Activated Charcoal Canisters (canisters) in conformance with 40 CFR, Part 61, Appendix B, Method 115, Restrictions to Radon Flux Measurements, (EPA, 20 16). These are passive gas adsorption sampling devices used to determine the flux rate of radon-222 gas from a surface. The canisters were constructed using a 10-inch diameter PVC end cap containing a bed of 180 grams of activated, granular charcoal. The prepared charcoal was placed in the canisters on a support grid on top of a ~ inch thick layer of foam and secured with a retaining ring under 1 Y2 inches of foam (see Figure 1, page 10). One hundred sampling locations were distributed throughout Cell 2 (consisting of one region) as depicted on the Sample Locations Map (see Figure 2, Appendix D). Each charged canister was placed 1 directly onto the surface (open face down) and exposed to the surface for 24 hours. Radon gas adsorbed onto the charcoal and the subsequent radioactive decay of the entrained radon resulted in radioactive lead-214 and bismuth-214. These radon progeny isotopes emit characteristic gamma photons that can be detected through gamma spectroscopy. The original total activity of the adsorbed radon was calculated from these gamma ray measurements using calibration factors derived from cross-calibration of standard sources containing known total activities of radium-226 with geometry identical to the counted samples and from the principles of radioactive decay. After approximately 24 hours, the exposed charcoal was transferred to a sealed plastic sample container (to prevent sample loss and/or further exposure during transport), identified and labeled, and transported to the Tellco laboratory in Grand Junction, Colorado for analysis. Tellco personnel maintained custody of the samples from collection through lab analysis. Upon completion of on-site activities, the field equipment was alpha and beta-gamma scanned by Energy Fuels Radiation Safety personnel for possible contamination resulting from fieldwork activities. All of the field equipment used was subsequently released for unrestricted use. A copy of the equipment release form is included in Appendix A. 5. FIELD OPERATIONS 5.1 Equipment Preparation All charcoal was dried at 11 ooc before use in the field. Unused charcoal and recycled charcoal were treated the same. 180-gram aliquots of dried charcoal were weighed and placed in sample containers. Proper balance operation was verified daily by checking a standard weight. The balance readout agreed with the known standard weight to within± 0.1 percent. After acceptable balance check, empty containers were individually placed on the balance and the scale was re-zeroed with the container on the balance. Unexposed and dried charcoal was carefully added to the container until the readout registered 180 grams. The lid was immediately placed on the container and sealed with plastic tape. The balance was checked for readout drift between readings. Sealed containers with unexposed charcoal were placed individually in the shielded counting well, with the bottom of the container centered over the detector, and the background count rate was documented. Three five-minute background counts were conducted on ten percent of the containers, selected at random to represent the "batch". If the background counts were too high to achieve an acceptable lower limit of detection (LLD), the entire charcoal batch was labeled non-conforming and recycled through the heating/drying process. 5.2 Sample Locations, Identification, and Placement On July 16, 2016, 100 sampling locations were spread out throughout the Cell 2 covered region. The approximate sampling locations that were established for previous samplings of Cell 2 were used for the placement of the canisters, although the actual sample identification numbers (IDs) are different. An individual ID was assigned to each sample point, using a sequential alphanumeric system indicating the charcoal batch and physical location within the region (e.g., FOl...FIOO). This ID was 2 written on an adhesive label and affixed to the top of the canister. The sample ID, date, and time of placement were recorded on the radon flux measurements data sheets for the set of one hundred measurements. Prior to placing a canister at each sample location, the retaining ring, screen, and foam pad of each canister were removed to expose the charcoal support grid. A pre-measured charcoal charge was selected from a batch, opened and distributed evenly across the support grid. The canister was then reassembled and placed face down on the surface at each sampling location. Care was exercised not to push the device into the soil surface. The canister rim was "sealed" to the surface using a berm of local borrow material. Five canisters (blanks) were similarly processed and these canisters were kept inside an airtight plastic bag during the 24-hour testing period. 5.3 Sample Retrieval On July 17, 2016 at the end of the 24-hour testing period, all canisters were retrieved, disassembled and each charcoal sample was individually poured through a funnel into a container. Identification numbers were transferred to the appropriate container, which was sealed and placed in a box for transport. Retrieval date and time were recorded on the same data sheets as the sample placement information. The blank samples were similarly processed. The charcoal from two of the samples (F36 and F73) was spilled during the canister retrieval process. The remaining charcoal samples from the Cell 2 covered region were successfully retrieved and containerized during the retrieval and unloading process. 5.4 Environmental Conditions A rain gauge and thermometer were placed at Cell 2 to monitor rainfall and air temperatures during sampling; additionally, Energy Fuels maintains an onsite rain gauge. In accordance with 40 CFR, Part 61, Appendix B, Method 115: • Measurements were not initiated within 24 hours of rainfall at the site. • There was no rainfall during the 24-hour sampling period. • All canister seals remained intact during the 24-hour sampling period. • The criteria regarding 35 degree F minimum ambient air temperature and unfrozen ground do not apply when performing sampling at multiple times throughout the year; however, the minimum air temperature during the 24-hour sampling period was 61 degrees F, and the ground was not frozen. 3 6. SAMPLE ANALYSIS 6.1 Apparatus Apparatus used for the analysis: • Single-or multi-channel pulse height analysis system, Ludlum Model 2200 with a Teledyne 3" x 3" sodium iodide, thallium-activated (Nai(Tl)) detector. • Lead shielded counting well approximately 40 em deep with 5-cm thick lead walls and a 7- cm thick base and 5 em thick top. • National Institute of Standards and Technology (NIST) traceable aqueous solution radium- 226 absorbed onto 180 grams of activated charcoal. • Ohaus Port-O-Gram balance with 0.1-gram sensitivity. 6.2 Sample Inspection and Documentation Once in the laboratory, the integrity of each charcoal container was verified by visual inspection of the plastic container. Laboratory personnel checked for damaged or unsealed containers and also checked that the data sheet was complete. Two containers (for samples F36 and F73) were empty because the charcoal from those samples was spilled during retrieval, as previously mentioned in Section 5.3 above, and therefore those two samples were deemed void. The remaining 98 sample containers and 5 blank containers inspected at the Tellco analytical laboratory were ultimately verified as valid with no damaged or unsealed containers observed. 6.3 Background and Sample Counting The gamma ray counting system was checked daily, including background and radium-226 source measurements prior to and after each counting session. Based on calibration statistics, using two sources with known radium-226 content, background and source control limits were established for each Ludlurn/Teledyne system with shielded counting well (see Appendix A). Gamma ray counting of exposed charcoal samples included the following steps: • The length of count time was determined by the activity of the sample being analyzed, according to a data quality objective of a minimum of 1,000 accrued counts for any given sample. • The sample container was centered on the Nal gamma detector and the shielded well door was closed. • The sample was counted over a determined count length and then the mid-sample count time, date, and gross counts were documented on the radon flux measurements data sheet and used in the calculations. • The above steps were repeated for each exposed charcoal sample. 4 • Approximately 10 percent of the containers counted were selected for recounting. These containers were recounted on the next day following the original count. 7. QUALITY CONTROL (QC) AND DATA VALIDATION Charcoal flux measurement QC samples included the following intra-laboratory analytical frequency objectives: • Blanks, 5 percent, and • Recounts, 10 percent All sample data were subjected to validation protocols that included assessments of sensitivity, precision, accuracy, and completeness. All method-required data quality objectives (EPA, 2016) were attained. 7.1 Sensitivity A total of five blanks were analyzed by measuring the radon progeny activity in samples subjected to all aspects of the measurement process, excepting exposure to the source region. These blank sample measurements comprised approximately 5 percent of the field measurements. Analysis of the five blank samples measured radon flux rates ranging from approximately 0.04 to 0.10 pCilm2-s, with an average of approximately 0.07 pCi/m2-s. The lower limit of detection (LLD) was approximately 0.06 pCilm2-s. 7.2 Precision Ten recount measurements, distributed throughout the sample set, were performed by replicating analyses of individual field samples (see Appendix B). These recount measurements comprised approximately 10 percent of the total number of samples analyzed. The precision of recount measurements, expressed as relative percent difference (RPD), for sample results above 1 pCilm2 -s ranged from less than 0.1 percent to 6.1 percent with an average precision of approximately 2.4 percent RPD. 7.3 Accuracy Accuracy of field measurements was assessed daily by counting two laboratory control samples with known Ra-226 content. Accuracy of these lab control sample measurements, expressed as percent bias, ranged from approximately -1.4 percent to + 1.2 percent. The arithmetic average bias of the lab control sample measurements was approximately -0.3 percent (see Appendix A). 7.4 Completeness Ninety-eight out of the total100 samples from the Cell2 cover region were verified, representing 98 percent completeness. 5 9. RESULTS 9.1 Mean Radon Flux Referencing 40 CFR, Part 61, Subpart W, Appendix B, Method 115 -Monitoring for Radon-222 Emissions, Subsection 2.1. 7 -Calculations, "the mean radon flux for each region of the pile and for the total pile shall be calculated and reported as follows: (a) The individual radon flux calculations shall be made as provided in Appendix A EPA 86(1). The mean radon flux for each region of the pile shall be calculated by summing all individual flux measurements for the region and dividing by the total number of flux measurements for the region. (b) The mean radon flux for the total uranium mill tailings pile shall be calculated as follows: J.tA1 + · · · hAd+l ... J!Ai At Where: Js =Mean flux for the Lotal pile (pCi/m2-s) Ji =Mean flux measured in region i (pCilm2-s) Ai =Area of region i (m2) At = Total area ofthe pile (m2)" 40 CFR 61, Subpart W, Appendix B, Method 115, Subsection 2.1 .8, Reporting states "The results of individual flux measurements, the approximate locations on the pile, and the mean radon flux for each region and the mean radon flux for the total stack [pile] shall be included in the emission test report. Any condition or unusual event that occurred during the measurements that could significantly affect the results should be reported." 7 9.2 Site Results Site Specific Sample Results (reference Appendix C) (a) The mean radon flux for the Ce112 region at the site is as follows: Cell 2 -Cover Region = 7.0 pCilm2-s (based on 270,624 m2 area) Note: Reference Appendix C of this report for the entire summary of individual measurement results. (b) Using the data presented above, the calculated mean radon flux for Cel12 is as follows: Cell2 = 7.0 pCi/m2-s (7.0)(270.624) = 7.0 270,624 As shown above, the arithmetic mean of the radon flux rate measurements representing the second half of the year 2016 for Cell 2 at Energy Fuels' White Mesa milling facility is below the U.S. Nuclear Regulatory Commission and EPA regulatory standard of 20 pCilm2 -s. Appendix C presents the summary of individual measurement results, including blank sample analysis. Sample locations are depicted on Figure 2, which is included in Appendix D. The map was produced by Tellco. 8 References U. S. Environmental Protection Agency, Radon Flux Measurements on Gardinier and Royster Phosphogypsum Piles Near Tampa and Mulberry, Florida, EPA 520/5-85-029, NTIS #PB86- 161874, January 1986. U. S. Environmental Protection Agency, Title 40, Code of Federal Regulations, July 2016. U. S. Nuclear Regulatory Commission, Radiological Effluent and Environmental Monitoring at Uranium Mills, Regulatory Guide 4.14, April1980. U.S. Nuclear Regulatory Commission, Title 10, Code of Federal Regulations, Part 40, Appendix A, January 2016. 9 Figure 1 Large Area Activated Charcoal Canisters Diagram fJGI!II( 10 lO-•n ~~ f'\ICEo~ r,.op Appendix A Charcoal Canister Analyses Support Documents A ENERGY FUELS RESOURCES WHITE MESA MILL, BLANDING, UTAH 2016 NESHAPs RADON FLUX MEASUREMENTS CELL2 SAMPLING DATES: 07/16/16-07/17/16 ANALYSIS DATES: 07/19/16-07/20/16 SYSTEM COUNT Bkg Counts (1 min. each) I.D. DATE #1 #2 M-01/D-21 7/19/2016 137 130 M-01/D-21 7/19/2016 126 142 M-01/D-21 7/20/2016 115 138 M-01/D-21 7/20/2016 142 110 M-01/D-21 7/19/2016 137 130 M-01/D-21 7/19/2016 126 142 M-01/D-21 7/20/2016 115 138 M-01/D-21 7/20/2016 142 110 M-02/D-20 7/19/2016 127 109 M-02/D-20 7/19/2016 110 131 M-02/D-20 7/20/2016 122 118 M-02/D-20 7/20/2016 108 128 M-02/D-20 7/19/2016 127 109 M-02/D-20 7/19/2016 110 131 M-02/D-20 7/20/2016 122 118 M-02/D-20 7/20/2016 108 128 #3 115 121 137 116 115 121 137 116 120 119 115 131 120 119 115 131 ACCURACY APPRAISAL TABLE JULY 2016 Source Counts (1 min. each) #1 #2 #3 10332 10274 10339 10216 10206 10279 10424 10292 10187 10246 10336 10386 10081 10074 10185 10142 10253 10117 10106 9990 10123 10271 10164 10172 10136 10172 10194 10166 10130 10232 9954 10151 10153 10238 10030 10065 10001 10253 10106 10120 10185 10041 10003 10024 10092 10168 10038 10034 AVG NET YIELD FOUND SOURCE cpm cpm/pCi pCi ID 10188 0.1698 59998 GS-04 10104 0.1698 59505 GS-04 10171 0.1698 59900 GS-04 10200 0.1698 60071 GS-04 9986 0.1698 58810 GS-05 10041 0.1698 59134 GS-05 9943 0.1698 58557 GS-05 10080 0.1698 59362 GS-05 10049 0.1697 59214 GS-04 10056 0.1697 59258 GS-04 9968 0.1697 58737 GS-04 9989 0.1697 58861 GS-04 10001 0.1697 58935 GS-05 9995 0.1697 58900 GS-05 9921 0.1697 58464 GS-05 9958 0.1697 58678 GS-05 AVERAGE PERCENT BIAS FOR ALL ANALYTICAL SESSIONS: KNOWN %BIAS pCi 59300 1.2% 59300 0.3% 59300 1.0% 59300 1.3% 59300 -0.8% 59300 -0.3% 59300 -1.3% I 59300 0.1% 59300 -0.1% 59300 -0.1% 59300 -0.9% 59300 -0.7% 59300 -0.6% 59300 -0.7% 59300 -1.4% 59300 -1.0% I I -0.3% J Energy Fuels Resmm.:cs (USA) Inc. White Mesa Mill Radintion Survey of Equipment Released for Unrestricted Use All equipment or material released f1om the White Mesa Mi!! to an unrestrict~~d area must b,~ surveyed for rdeasl~ in aceord<mc(' with the following procedure. L Monitm for Gross alpha cont<imiMtion with the appropriate survey meter. 7 If caku!at~d <i$Say exceeds 1,000 dpmi lOOcm", then perfQrm swipi' analysis a! applicable point;. 3. Decontaminate if a mmovub!e nlpha exceeds l ,000 dpm/Hl0cm2 or fixed alpha exct~eds 5,000 dpm/100cm2. 4. Release equipment or material if u!pha contnmin:Hion and Dt:ta-Gamrna le\cls nre bdow the fo!l,wing limit: R!!-movnhlc alph£\ --1,000 dpm/ I ()0cm2 r:ixcd alpha-5,000 dpnvl00cm2 nvcruge 15,000 drmll OOcn/ mnximum Betn·Garnma-0.2 mr/ht·@ !em avt:ragt: LO mr!hr@ Jcm nsaxirnum l .ist of Equipment Total Alpha dpmilOOcm-Removable Atrha Beta/Gamma mr/lu dem/IOOcm 9-"-l wA~:~krJ z. 5 J"if.es·-ei/V..~tJ J, J ·-bcx .54MIJ (~ ·1. i -· ~ C'i·~ d f~,.,m.f; "·~}Y $wcotA ~Jce_c; Instr um.:nt Function checks Alpha Meter: Inst. Model 3 SN :1 3 5.28'3 Th-2~0 Sourc~ SN 03Jl(~o'l..- dpm l G,ft 0 Jllll )[(JO df 7-6 0'/o Efliciency Pactor 12-· '3 Cnl. Dutc: 2 7111ay...Lk~~.-_ Bke :2o MDA :29() S..BKG ~m .:.~ B/C6 <::.·8, ---lj?6 -!-~ BK6 ..--5 0{07 -~-;:;. r.'~ 08' -... -~-" ~ 0.18 ------,c' 'i? -0.0(. y----~-D·,.o5 Removable Alpha: Inst. Modd __ -:--.--1"'~~---- dpm ____ cp 1.,_~-+- Efficicncy Factor_,_ __ Cal. Datt!: .. _. ___ _ CHARCOAL CANISTER ANALYSIS SYSTEM siTE LocATION= 'W 6",--t-.e. fV\~s"' M i H} B 1 P\t'\ J \YlDj J U T cuENT: E-Y\~~1 F'-(e\s ResoLI\.CC..-i'5 {V\.SA) Calibration Check Lou System ID: _tJ\_-_0_,_/ _ _,D=----· _'2-_\ __ Calibration Date: '7/l 'i J I 'e Due Date: I J j 'i J I 7 Scaler SIN: __ S:~..:....I ""'5~'1.........-=::L=---High Voltage: l I (,G) Window: 4.42 Thrshld: 2.20 Detector SIN: --=O_Li..:._..;.' ...,So::........:3::=;.....3~--Source 10/SN: ~"l-:z,.~ J.. I G S ~ D'/ Source Activity: -5") • "3 ~ pt.: Blank Canister Bkgd. Range, cpm: 2 a= f06 to lvJ 3a= ~Lf to ''~ Gross Source Range, cpm: 2o~ <10)'-1/ ., JD't5l'"" 'lSoq Technician: "2:;) Z Q2 q,c= All counts llmes are one minute to IOS"Ss- Date By Background Countsjl min. each) Source Counts (I min. each) ok? #1 #2 #3 Avg. #1 #2 #3 Average YIN '7/IOJ/1{, y~ \ ~ 7 \ 0 liS 1'")./ 103~").. I 0·.2.74 IOL,'~G I 0'3 )5 'I_ "'1/Jf~/1 C, TJJJ-12-(, i L{ :l \ ::2.. I l '30 l 0 :J...H.. t0"2..o (,; l 0-2, ~ I 0'2._ ~ 4 \1 li/2b/lt,. I7Z£. 115 \ H:S 13'7 r~O IOY:l-., 10'2.01"2.. tOlf61 · o~OJ \I_ 7/WIJ/117.~ I 4~ t \0 i I~ l "l-'3 tO~"fr, \0":1,~(. I0"3f\lo I 0~'2-~ ..t./ ~llf.~'l.. 1~71\~ \11 11...1-t 1010 l01€Lit~.t;'-~_t_02'f" Y 1'7J"ZJ/'(, r/:~ JO~ \"3_5 1"2. J')..."'2.J0'375 \01~"1 10200 10~5-"1 Y 1-1h!:zl1"' ~ llw ~"3~ 1"2-B i'l.B J03f3'i .o·2-'?e ,o.3t'3 ID33S v '7~-,'tc..ll7L-t'--13~ lOR \2'2. \")...1 i0210 JOtt.lb t00,_'7-10i'i'3 :.t YIN: Y ~average background and source cpm falls within the control limits. N = average background and source cpm does not fall within the control limits. The acceptable ranges were determined from prior background and source check data. CHARCOAL CANISTER ANALYSIS SYSTEM siTEwcATroN: W h.\ -e M.e...s~ N\'. \\. B lt?tVl J ~ ..-tlj J \AI cLIENT: E.. n -er~'j F \A -e \s 'R ~so"'-r c....~ s (us A) Calibmtjon Check l.og System 10: -'--tv\_,_---=-0_\,_,,,_/_.D~--=2..=..\,_ __ Calibration Date: 7 J l'"t J J Ca Due Date: -,j J l.f J I l • Scaler SIN: __ 5,;__1....:;:5::;..__/~2:::........ ___ High Voltage: I I G:, C) Window: 4 42 Thrshld: 2.20 Detector SIN: ---=O'-'f-=--=1 __ 5=-'?>..:;;.._;:3:;;..._ __ Source ID/SN: ~ "'2.'2-i-!Gr S --OS Source Activity: 5 ~ • 3 to(. f C.. ; Blank Canister Bkgd. Range, cpm: 2 a= l06 to l~l 3a= 9 Lf to l!Lf 0)")00) to I 0'-tG}"l-3 a= Tec!mician: ----;-MP~k~tv~~'--='------0Ji~&~3 to f0t:;.'36 Gross Source Range, cpm: 2a• All counts times arc one minute Date By Backg ound Counts (l min. each) Source Counts (l min. each) ok7 #1 #2 #3 Avll. #1 #2 #3 Average YIN YIN: Y =average background and source cpm falls within the control limits. N -= average background and source cpm does not fall within the control limits. The acceptable ranges were determined from prior background and source check data. CHARCOAL CANISTER ANALYSIS SYSTEM SITE LOCATION: W h·,+.(, \'\\eSt:>\ M; \\, BJ~~d.~ YIQ_) ~ CLIENT: £. n -t r'j'j F Vi e 15 }2. ~ so ~.-.r~ s (\.A. S A) Ca!jbmtjon Check Log System ID: ~ -0~./ 'D ·-:J-0 Calibration Date: 7/ I 4 /I (., Due Date: "1/14/1 I Scaler SIN: S I 5 V 3 High Voltage: "2.5 Window: 4.42 Thrshld: 2.20 Detector SIN: 0 41 53 :L. Source ID/SN: RGi"Z2.VG-s -o'f Source Activity: c;"") :"3 t'-p (.i Blank Canister Bkgd. Range, cpm: 2 cr = I 0 ').. to I (p) 3 cr = ~~ to 17 f3 GrossSourceRange,cpm: 2cr= C)O) 50 to (04S '"3 3 cr= 0) 8"2..$ to I 057 8 Technician: 12 L {'.,o--s.p= All counts times are one minute Date By BackJl: -ound Counts (I min. each_) Source Counts Jl min. each) ok? #I #2 #3 Avg. #I #2 #3 Average YIN 7 10)/ lv 1/tC... 1'2.""7 lOClJ \7-0 ll q lo I ~l. lOll ::L \0 lCf4 I 0 I ID"1 V 7.ftq 'I~ 17).4 UO 1"31 \\_'\ '"l.O 1DL"-(, 101~ lO'-~, 10 1it., 'v 7:to/J, inL 1"2-7-lt_ts 1\~ tLS ~«J.5~ \O'C'J l0l~3_ tODB(, ~ 1""112o/IG, P)£ \oB 1"'2.5 1"3 ,-z.,..-...tO'l..~A \0030 \00(..'<" LOl I l 'Y 7~,.hc. DU. \\\ \\4 lOrn alO tO\~S \0"2-<"1 0)98C. 'Ol~'i ~ """l"l..Ut/. ~1-L 14-_ 1114 13.!) _l')..l-\OQP,O lOlq~ ~01")0 _tOJS"S -../ '7 '21-)/Y -:n.e_. '0.~ l '2.. '? \ 'i7 I ").Ji t0""'2..P}O} \O_ea~ IOO 3S' _10 \4 ~ 'I 17/2.2./J" PU. 1'2.."2.. \Q7 1~3 1""'2-l lDOBS LD~lt,'J. lO'l.lo ~0\SI ~ YIN: Y =average background and source cpm falls within the control limits. N =-average background and source cpm does not fall within the control limits. The acceptable ranges were determined from prior background and source check data. CHARCOAL CANISTER ANALYSIS SYSTEM Calibration Check Log System ID: ____,t/\___:_---=.0......;;2__,_/_V~_-.::...2-._D__ Calibration Date: 7/1 "f J I Y Scaler SIN: 5 I 5 (, 3 High Voltage: l3'2...$ Window: Detector SIN: 0 LJ l 5 "31-Source ID/SN: ~"'"Z.~ if(, S · · OS Blank Canister Bkgd. Range, cpm: 2 u "' I 0 "2. to i ~ '3 3 a= Gross Source Range, cpm: 2 a= 0) C) '? V to I 0'-t 5 I 3 a= Technician: X2Z---~ All counts times are one minute Due Date: 7/ I '-f / IJ 4.42 Thrshld: 2.20 Source Activity: 50) • 3 ~ f L; B7 to l--? 8 "Bol to r osgo Date By Back~ ound Counts (l min. each) Source Counts ll min. each) ok? #1 #2 #3 Avg. #l #2 #3 Averal!e YIN '1 'All~ nL l ""1-1 lOCI 1'2.0 l I q I 000 I ~~ 10 tOt... t0\~0 -..{__ 1-ilto,/lli ~ 110 I~ 1 I~ \"'2...£J I 0 1"21) \t':>l ~<"' l0£?41 I 0 II~ 'V 1"7 l'lOIJ~ ~ l '2...'"1-l \I=! 1 I~ 1 \ S 1 ()(){) ~ I 062L1 11'1t?oi "2 I OOCfO V ., '7..61 ~~~ :?2£ 1 o ~ 1 ')..1 r , '"':\ J , L.. "-" \-,") , c, (1, 1 oo"'\~ It~ t oo A o -v !"f/'2J/tt. ~ l l I i I c. 1 Qt, 1 10 !0:2-lo1 lOll~ .G\0)":2,~ rOt 01 ''-L 1'1~7-//tv g--a, Jt.t; 11L. ~~~ ,~,_ I003\ ~Q)ifLt?; tDL.J~ -1oo·7·, "'" I 7h.::1/ ItA !'XL 'oc:-r'2."' a47 \ "'Z..S 1 &}q~ 1 1 Ol"'l-1 1 O:l-'-1-::l 101 o l ~' 1. ~~~,_ i/~L f "2.~ i 01 I ~"";l I~\ tO 0£..1 "'2. I 0"2...~ t 0 I 7;.0: I 0 T::g:: ~ ...J r YIN: Y"' average background and source cpm falls within the control limits. N "' average background and source cpm does not fall within the control limits. The acceptable ranges were determined from prior background and source check data. BALANCE OPERATION DAILY CHECK Balance Model: Q h (it V\ S -r Of"-\ -0 -<1 (''1 W' S ,t.J, ~ l "'2. 3 0 l Standard Weight (g): "3 0 0 , 0 'fi , Date Pre-check (g) Post-check (g) O.K. :t 0.1%? By ...,,,~,,, 3 o_,, 0 '3 oo. 0 '/_~s I ~ ..., /""}..0 /I " 300,0 300,0 \}e .~ !l>L~~ -,j;;..l/t(p ' .VLa:,~ 300.0 300.·0 ve.s 1/?-~/ IL, ;;z. ~ C3."' -;z.q~,q 'v~s bL4~.- I AppendixB Recount Data Analyses B CLIENT: ENERGY FUELS RESOURCES PROJECT: RADON FLUX MEASUREMENTS, WHITE MESA MILL PILE: 2 BATCH: F SURFACE: SOIL AIR TEMP MIN: 61°F AREA: COVER DEPLOYED: 7 16 16 RETRIEVED: 7 17 16 CHARCOAL BKG: FIELD TECHNICIANS: CE,DLC, WM, GK COUNTED BY: DLC DATA ENTRY BY: DLC COUNTING SYSTEM I.D.: M01/D21, M02/D20 CAL. DUE: 7/14/17 RECOUNT CANISTER ANALYSIS: PROJECT NO.: 16004.03 WEATHER: CLEAR, NO RAIN 139 cpm Wt. Out: TARE WEIGHT: 180.0 29.2 g. g. GRID SA!>fPLE RETRIV AW\.LYSIS ZHD-TH!E CNT GROSS GROSS RADON ± LLD PRECISION LOCATION I. D. HR MIN HR MIN MO DA YR HR MIN (MIN) COUNTS WT IN pCi/m2 s pCi/m2 s pCi/m2 E! % RPD FlO RECOUNT F20 RECOUNT F30 RECOUNT F40 RECOUNT F50 RECOUNT F60 RECOUNT F70 RECOUNT F80 RECOUNT F90 RECOUNT FlOO RECOUNT FlO FlO F20 F20 F30 F30 F40 F40 FSO F50 F60 F60 F70 F70 F80 F80 F90 F90 FlOO FlOO 7 12 7 14 7 19 16 17 16 7 12 7 14 7 20 16 17 26 7 42 7 3 0 7 19 16 17 26 7 42 7 30 7 20 16 17 27 7 12 7 26 7 19 16 17 39 7 12 7 26 7 20 16 17 30 7 57 7 37 7 19 16 17 47 7 57 7 37 7 20 16 17 31 7 12 7 13 7 19 16 18 3 7 12 7 13 7 20 16 18 34 7 45 7 24 7 19 16 18 15 7 45 7 24 7 20 16 18 33 7 12 7 14 7 19 16 18 24 7 12 7 14 7 20 16 18 36 7 44 7 27 7 19 16 18 31 7 44 7 27 7 20 16 18 36 7 57 7 32 7 19 16 18 43 7 57 7 32 7 20 16 18 38 1 1 2 2 1 1 2 2 2 2 1 1 1 1 1 1 1 1 2156 217.8 1817 217.8 1812 217.6 1543 217.6 5533 224.3 4684 224.3 1921 226.6 1678 226.6 1871 214.0 1507 214.0 8376 213.3 6941 213.3 1725 217.6 1445 217.6 3226 209.9 2647 209.9 1313 213.9 1121 213.9 4.4 4.4 1.7 1.7 11.7 11.9 1.8 1.9 1.7 1.6 18.3 18.2 3.5 3.5 6.9 6.7 2.6 2.7 0.4 0.4 0.2 0.2 1.2 1.2 0.2 0.2 0.2 0.2 1.8 1.8 0.4 0.4 0.7 0.7 0.3 0.3 0.04 0.05 0.04 0.05 0.04 0.05 0.04 0.05 0.04 0.05 0.04 0.05 0.04 0 .05 0.04 0.05 0.04 0.05 7 59 7 30 7 19 16 18 56 1 2877 215.0 6.2 0.6 0.04 7 59 7 30 7 20 16 18 38 1 2514 215.0 6.4 0.6 0.05 AVERAGE PERCENT PRECISION FOR THE CELL 2 COVER REGION: Page 1 of 1 0.0% 0.0% 1. 7% 5.4% 6.1% 0.5% 0.0% 2.9% 3.8% 3.2% 2.4% Appendix C Radon Flux Sample Laboratory Data (including Blanks) c CLIENT: ENERGY FUELS RESOURCES PROJECT: RADON FLUX MEASUREMENTS, WHITE MESA MILL PILE: 2 BATCH: F SURFACE: SOIL AREA: COVER DEPLOYED: 7 16 16 RETRIEVED: 7 COUNTED BY: DLC FJELD TECHNICIANS: CE,DLC, WM, GK COUNTING SYSTEM J.D.: M01/D21, M02/D20 CAL. DUE: 7/14/17 AIR TEMP MIN: 61°F 17 16 CHARCOAL BKG: DATA ENTRY BY: DLC PROJECT NO.: 16004.03 WEATHER: CLEAR, NO RAIN 139 cpm Wt Out TARE WEIGHT: 180.0 29.2 GRID Sl<MPLE DEPLOY RETRIV ANALYSIS MID-TIHE CNT GROSS GROSS RADON t LLD g. g. LOCATION I. D. ~R MIN HR MIN l·lO DA YR HR MIN (MIN) COUNTS WT IN pCi/m> 6 pCi/m2 s pCi/m2 6 COMMENTS: FOl F02 F03 F04 F05 F06 F07 FOB F09 FlO F11 F12 F13 F14 F15 F16 F17 F18 F19 F20 F21 F22 F23 F24 F25 F26 F27 F28 F29 F30 F31 F32 F33 F34 F35 F36 F37 F38 FOl F02 F03 F04 F05 F06 F07 FOB F09 FlO Fll F12 F13 F14 F15 F16 F17 FlB F19 F20 F21 F22 F23 F24 F25 F26 F27 F28 F29 F30 F31 F32 F33 F34 F35 F36 F37 F38 6 45 6 48 6 51 6 54 6 57 7 0 7 3 7 6 7 9 7 12 7 15 7 18 7 21 7 24 7 27 7 30 7 33 7 37 7 39 7 42 6 45 6 48 6 51 6 54 6 57 7 0 7 3 7 6 7 10 7 10 7 11 7 11 7 12 7 12 7 13 7 13 7 14 7 14 7 15 7 15 7 16 7 34 7 35 7 36 7 37 7 29 7 29 7 30 7 22 7 22 7 23 7 23 7 24 7 24 7 25 7 25 7 9 7 26 7 12 7 26 7 15 7 27 7 lB 7 27 7 21 7 41 7 24 7 40 7 27 7 39 7 29 7 48 7 35 7 51 7 36 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 10 10 11 11 13 13 14 14 16 16 17 17 19 19 20 20 22 23 26 26 30 30 33 32 36 36 37 37 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 2 3 2 3 3 3 1 1 1 1 1 2255 1808 3011 6119 2466 1928 7789 3045 1676 2156 13710 3754 3006 43B2 4280 3762 11986 1061 1088 1B12 1347 1212 1304 1033 1081 1247 3419 1926 225.8 220.4 219.2 222 .9 223.5 225.1 216.3 218.3 217.4 217.8 216.2 215.0 220.0 217.3 216.6 214.7 211.1 215.2 227.2 217.6 225.8 226.4 219.2 229.6 222.9 224.1 225.0 234.4 7 19 16 17 39 1 3667 237.3 7 19 16 17 39 1 5533 224.3 7 19 16 17 40 1 15459 192.1 7 19 16 17 40 1 3345 226.9 7 19 16 17 42 1 12395 211.1 7 19 16 17 42 1 18789 213.5 7 19 16 17 43 1 5978 222.1 VOID -SAMPLE SPILLED DURING RETRIEVAL 7 19 16 17 45 1 3310 225.3 7 19 16 17 45 1 1394 212.7 Page 1 of 3 4.6 3.6 6.2 13.0 5.1 3.9 16.7 6.4 3.4 4.4 29.9 B.O 6.3 9.3 9.0 7.9 25.9 0.9 0.5 1.7 0.7 0.6 0.6 1.9 2.0 2.4 7.1 3.9 7.7 11.8 33.5 7.0 26.6 40.6 12.8 7.0 2.8 0.5 0.4 0.6 1.3 0.5 0.4 1.7 0.6 0.3 0.4 3.0 O.B 0.6 0.9 0.9 0.8 2.6 0.1 0.1 0.2 0.1 0.1 0.1 0.2 0.2 0.2 0.7 0.4 0.8 1.2 3.3 0.7 2.7 4.1 1.3 0.7 0.3 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 CLIENT: ENERGY FUELS RESOURCES PROJECT: RADON FLUX MEASUREMENTS, WHITE MESA MILL PILE: 2 BATCH: F SURFACE: SOIL AREA:COVER DEPLOYED: 7 16 16 RETRIEVED: 7 COUNTED BY: DLC FIELD TECHNICIANS: CE,DLC, WM, GK COUNTING SYSTEM I.D.: M01/D21, M02/D20 CAL. DUE: 7/14/17 AIR TEMP MIN: 61 °F 17 16 CHARCOAL BKG: DATA ENTRY BY: DLC PROJECT NO.: 16004.03 WEATHER: CLEAR, NO RAIN 139 cpm Wt. Out TARE WEIGHT: 180.0 29.2 GRID SAMPLE DEPLOY RETRIV ANALYSIS MID-TIHE CNT GROSS GROSS RADON ± LLD g. g. LOCATION I. D. HR ZUN HR MIN MO DA YR HR MIN (!UN) COUNTS liT IN pCi/m's pCi/m's pCi/m2 s CONMENTS : F39 F40 F41 F42 F43 F44 F45 F46 F47 F48 F49 F50 F51 F52 F53 F54 F55 F56 F57 F58 F59 F60 F61 F62 F63 F64 F65 F66 F67 F68 F69 F70 F71 F72 F73 F74 F75 F76 F39 F40 F41 F42 F43 F44 F45 F46 F47 F48 F49 F50 F51 F52 F53 F54 F55 F56 F57 F58 F59 F60 F61 F62 F63 F64 F65 F66 F67 F68 F69 F70 F71 F72 F73 F74 F75 F76 7 54 7 57 6 45 6 48 6 51 6 54 6 57 7 0 7 3 7 6 7 9 7 12 7 15 7 21 7 24 7 27 7 30 7 35 7 38 7 40 7 43 7 45 6 45 6 48 6 51 6 54 6 57 7 0 7 36 7 37 7 10 7 10 7 10 7 11 7 11 7 11 7 12 7 12 7 12 7 13 7 13 7 14 7 14 7 14 7 15 7 20 7 21 7 22 7 23 7 24 7 10 7 10 7 11 7 11 7 12 7 12 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 17 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 7 19 16 18 47 47 50 49 53 53 56 55 59 0 2 3 5 5 8 8 11 11 13 13 15 15 17 17 19 19 21 21 2 2 3 1 2 2 2 1 1 2 1 2 2 1 3 1 2 1 1 1 1 1 2 2 1 1 1 1 1211 1921 1248 7145 1374 1559 1655 3343 8139 1878 2230 1871 1272 1092 1302 1659 1811 6937 2465 6516 4732 8376 1122 1003 1037 2393 1859 3135 220.4 226.6 212.7 217.1 220.0 216.0 224.1 219.5 223.3 214.1 214.6 214.0 216.4 234.3 217.3 220.0 220.8 208.4 210.5 214.1 213.6 213.3 211.5 222.2 222.5 225.3 213.5 220.4 7 3 7 13 7 19 16 18 22 1 5363 217.5 7 6 7 13 7 19 16 18 22 1 5880 218.5 7 9 7 14 7 19 16 18 24 1 1001 220.4 7 12 7 14 7 19 16 18 24 1 1725 217.6 7 15 7 15 7 19 16 18 25 1 1679 215.4 7 18 7 15 7 19 16 18 25 1 2822 224.5 7 21 VOID -SAMPLE SPILLED DURING RETRIEVAL 7 24 7 16 7 27 7 17 7 32 7 23 7 19 16 18 7 19 16 18 7 19 16 18 27 28 28 1 1 1 Page 2 of 3 1022 1710 2545 218.5 231.2 209.4 1.0 1.8 0.6 15.3 1.2 1.4 1.5 7.0 17.6 1.8 4.6 1.8 1.1 2.1 0.7 3.4 1.7 15.2 5.2 14.3 10.3 18.5 0 .9 o.a 2.0 4.9 3 .8 6 .6 11.5 12.7 1.9 3.5 3.4 6 .0 2.0 3.5 5.4 0.1 0.2 0.1 1.5 0.1 0.1 0.2 0.7 1.8 0.2 0.5 0.2 0.1 0.2 0.1 0.3 0.2 1.5 0.5 1.4 1.0 1.8 0.1 0.1 0.2 0.5 0.4 0.7 1.2 1.3 0.2 0.4 0.3 0.6 0.2 0.4 0.5 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 CLIENT: ENERGY FUELS RESOURCES PROJECT: RADON FLUX MEASUREMENTS, WHITE MESA MILL PILE: 2 BATCH: F SURFACE: SOIL AIR TEMP MIN: 61°F AREA: COVER DEPLOYED: 7 16 16 RETRIEVED: 7 17 16 CHARCOAL BKG: FIELD TECHNICIANS: CE,DLC, WM, GK COUNTED BY: DLC DATA ENTRY BY: DLC COUNTING SYSTEM I.D.: M01/D21, M02/D20 CAL DUE: 7/14/17 PROJECT NO.: 16004.03 WEATHER: CLEAR, NO RAIN 139 cpm Wt. Out: TARE WEIGHT: 180.0 29.2 GRID SA..'I1PLE DEPLOY RETRIV .P-.NALYSIS MID-Tit-lE CNT GROSS GROSS RADON ± LLD g. g. LOCATION I . D. HR MIN HR MIN lo!O DA YR HR MIN (MIN) COUNTS WT IN pCi /m' s pCi /m' s pCi /m' s COMMENTS: F77 F78 F79 F80 F81 F82 F83 F84 F85 F86 F87 F88 F89 F90 F91 F92 F93 F94 F95 F96 F97 F98 F99 F77 F78 F79 F80 F81 F82 F83 F84 F85 F86 F87 F88 F89 F90 F91 F92 F93 F94 F95 F96 F97 F98 F99 F100 F100 BLANK CANISTER ANALYSIS: 7 35 7 38 7 41 7 44 7 47 7 50 7 53 7 56 7 59 7 45 7 48 7 51 7 54 7 57 7 34 7 36 7 39 7 42 7 45 7 48 7 51 7 54 7 57 7 24 7 19 16 18 7 25 7 19 16 18 7 26 7 19 16 18 7 27 7 19 16 18 7 29 7 19 16 18 7 30 7 19 16 18 7 31 7 19 16 18 7 32 7 19 16 18 7 33 7 19 16 18 7 30 7 19 16 18 7 31 7 19 16 18 7 31 7 19 16 18 7 32 7 19 16 18 7 32 7 19 16 18 7 33 7 19 16 18 7 33 7 19 16 18 7 34 7 19 16 18 7 34 7 19 16 18 7 35 7 19 16 18 7 25 7 19 16 18 7 27 7 19 16 18 7 28 7 19 16 18 7 29 7 19 16 18 30 30 31 31 34 34 37 37 40 40 42 42 43 43 45 45 47 47 49 49 53 53 56 1 1 1 1 2 3 3 2 1 1 1 1 1 1 1 1 2 1 1 2 3 3 2 3087 1076 1550 3226 1362 1005 1181 1123 3037 1607 9286 7068 8452 1313 6365 1145 1388 12790 4383 1002 1011 1009 1184 212.7 211.0 208.1 209.9 215.4 219.1 211.7 213.2 215.1 214.0 216.6 212.9 212.0 213.9 214.1 214.6 217.2 225.0 171.1 210.9 216.0 210.8 212.3 7 59 7 30 7 19 16 18 56 1 2877 215.0 AVERAGE RADON FLUX RATE FOR THE CELL 2 COVER REGION: 6.6 2.1 3.2 6.9 1.2 0.4 0.6 1.0 6.5 3.3 20.5 15.6 18.7 2.6 13.8 2.2 1.2 28 .2 9 .5 0 .8 0 .4 0 .4 1.0 0.7 0.2 0.3 0.7 0.1 0.1 0.1 0.1 0.7 0.3 2.1 1.6 1.9 0.3 1.4 0.2 0.1 2.8 0.9 0.1 0.1 0.1 0.1 0.04 0.04 0.04 0.04 0 .04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 6.2 0.6 0.04 7.0 pCi/m2 s OA-MIN 40.6 MAX GRID SAMPLE RETRIV ANl>.LYSIS HID-TIME CNT GROSS GROSS RADON ± LLD LOCATION I. D. HR MIN HR MIN MO DA YR HR MIN (MIN) COUNTS WT IN pCi/m' a pCi/m' s pCi/m' s CO~NTS: F BLANK 1 F BLANK 2 F BLANK 3 F BLANK 4 F BLANK 5 F BLANK 1 6 30 F BLANK 2 6 30 F BLANK 3 6 30 F BLANK 4 6 30 F BLANK 5 6 30 7 15 7 19 16 19 5 7 15 7 19 16 19 5 7 15 7 19 16 19 16 7 15 7 19 16 19 16 7 15 7 19 16 19 28 10 10 10 10 10 1853 1579 1766 1614 1575 206.9 210.3 206.6 208.9 209.9 AVERAGE BLANK CANISTER ANALYSIS POR THE CELL 2 COVER REGION: Page 3 of 3 0.10 0.04 0.08 0.05 0.04 0.06 0.03 0.03 0.03 0.03 0.03 pCi/m2 s 0 .04 0.04 0 .04 0.04 0.04 CONTROL CONTROL CONTROL CONTROL CONTROL AppendixD Sample Locations Map (Figure 2) D -cELL 1- __,.... o-o ,., , .. .... ... F07 0 0 0 0 0 0 0 F21 F22 F23 F24 F25 F26 m 0 ...c!MOONSIIIICnOI<---"' 0 ,., 0 0 ... 0 -cELL2-,., 0 '"' 0 F46 0 0 F47 F6S 0 F66 0 F67 ,., 0 -au.• F34 F3S 0 0 ,,. f57 F58 FS9 F60 0 0 0 0 0 "\ ~ "' F77 F78 F79 FBO 0 0 0 0 0 -CEU.2- F87 F86 F20 F19 F18 . \\ 0 0 0 0 0 F6S f84 F83 F82 FBI 0 0 0 0 0 .~ l' I I I • I I Wt!ITE MESA MIL!. BLANDING. UTAH NESHAPS 20_16 JULY 2016 SAMPLING 7/16/15-7/17/16 PREPARED FOR ENERGY FUELS RESOURCES Wi&llQ F01 0 • SAMPLE lOCATION ON COVERED AREAS FIGURE 2 " t ~Elttrtrf 4i4 ltiO ICO 0 lOO ,,,,,. ENVJRONMENTAL. U.C ~m~~~ ""' fVIIIOOVC£O, ~OII'USEDf'O.Nff C1IIU PIIOJ<CTOA f)(-011>f$1'11CW:T EXCEPT n AGflfEMlHT .... 'fTHlD..lCO.