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HomeMy WebLinkAboutDRC-2012-002406 - 0901a06880326108-2012-002406 ENERGYFUELS Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www energyfitels com November 27, 2012 Sent VIA OVERNIGHT DELIVERY Mr Rusty Lundberg Director Division of Radiation Control Utah Department of Environmental Quality 195 North 1950 West PO Box 144850 Salt Lake City, UT 84114-4820 '1 Re: Transmittal of 3rd Quarter 2012 Routine Chloroform Monitoring Report UDEQ Docket No. UGW-20-01- White Mesa Uranium Mil! Dear Mr Lundberg Enclosed are two copies of the White Mesa Uranium Mill Chloroform Monitoring Report for the 3rd Quarter of 2012 as required by the Notice of Violation and Groundwater Corrective Action Order, UDEQ Docket No UGW-20-01 as well as two CDs each containing a word searchable electronic copy of the report If you should have any questions regardmg this report please contact me Yours very truly, . ENERGY FUELS RESOURCES (USA) INC Jo Ann Tischler Director, Compliance CC. David C Frydenlund Harold R Roberts David E Turk _ KathenneA Weinel Central Files November 27,2012 Sent VIA OVERNIGHT DELIVERY Mr. Rusty Lundberg Director Division of Radiation Control Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144850 Salt Lake City, UT 84114-4820 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 3039742140 www.energyfuels.com Re: Transmittal of 3rd Quarter 2012 Routine Chloroform Monitoring Report UDEQ Docket No. UGW-20-01-White Mesa Uranium Mill Dear Mr. Lundberg: . Enclosed are two copies of the White Mesa Uranium Mill Chloroform Monitoring Report for the 3rd Quarter of 2012 as required by the Notice of Violation and Groundwater Corrective Action Order, UDEQDocket No. UGW -20-01 as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours very truly, . ~~ ENERGY FUELS RESOURCES (USA) INC. Jo Ann Tischler Director, Compliance cc: David C. Frydenlund Harold R. Roberts David E. Turk Katherine A. Weinel Central Files White Mesa Uranium Mill Chloroform Monitoring Report State of Utah Notice of Violation and Groundwater Corrective Action Order UDEQ Docket No. UGW-20-01 3rd Quarter (June through September) 2012 Prepared by: Energy Fuels Resources (USA) Inc. 225 Union Boulevard, Suite 600 Lakewood, CO 80228 November 27,2012 TABLE OF CONTENTS 1.0 INTRODUCTION ................................................................................................. 1 1.1 Groundwater Discharge Permit Modifications during the Quarter. .................... 1 2.0 CHLOROFORM MONITORING ............................. $0 ....................................... 1 2.1 Samples and Measurements Taken During the Quarter ..................................... 1 2.1.1 TW4-27 .............................................................................................................. 1 2.1 ~2 Chloroform Monitoring ..................................................................................... 2 2.1.3 Parameters Analyzed .................................................................................. 2 2.1.4 Groundwater Head Monitoring ................................................................... 3 2.2 Sampling Methodology and Equipment and Decontamination Procedures ....... 3 2.2.1 Well Purging and Depth to Groundwater ................................................... 4 2.2.2 Sample Collection ....................................................................................... 5 2.3 Field Data ............................................................................................................ 6 2.4 Depth to Groundwater Data and Water Table Contour Map .............................. 6 2.5 Laboratory Results ............................................................................................... 6 2.5.1 Copy of Laboratory Results ........................................................................ 6 2.5.2 Regulatory Framework ............................................................................... 6 3.0 QUALITY ASSURANCE AND DATA VALIDATION ................................... 6 3.1 Field QC Samples ............................................................................................... 7 3.2 Adherence to Mill Sampling SOPs ..................................................................... 7 3.3 Analyte Completeness Review ........................................................................... 8 3.4 Data Validation ................................................................................................... 8 3.4.1 Field Data QA/QC Evaluation .................................................................... 8 3.4.2 Holding Time Evaluation ............................................................................ 9 3.4.3 Receipt Temperature Evaluation ............................................................... 10 3.4.4 Analytical Method Checklist .................................................................... 10 3.4.5 Reporting Limit Evaluation ...................................................................... 10 3.4.6 Receipt pH Evaluation .................................................................................. 10 3.4.7 Trip Blank Evaluation ............................................................................... 11 3.4.8 QAlQC Evaluation for Sample Duplicates· ............................................... 11 3.4.9 Rinsate Sample Check .............................................................................. 11 3.4.10 Other Laboratory QAlQC ......................................................................... 12 4.0 INTERPRETATION OF DATA ....................................................................... 13 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions ........... 13 4.1.1 Current Site Groundwater Contour Map ................................................... 13 4.1.2 Comparison of Current Groundwater Contour Maps to Groundwater Contour Maps for Previous Quarter ......................................................... 15 4.1.3 Hydrographs .............................................................................................. 15 4.1.4 Depth to Groundwater Measured and Groundwater Elevation ................. 15 4.1.5 Evaluation of the Effectiveness of Hydraulic Capture ............................ 16 4.2 Review of Analytical Results ............................................................................ 17 4.2.1 Current Chloroform Isoconcentration Map .............................................. 17 4.2.2 Chloroform Concentration Trend Data and Graphs .................................. 17 4.2.3 Interpretation of Analytical Data .............................................................. 17 5.0 LONG TERM PUMP TEST AT MW-4, MW-26, TW4-19, TW4-20, AND TW 4-4 OPERATIONS REPORT ..................................................................... 18 N:\ WMM\Required Reports\Chloroform Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroform _Report _text. doc 5.1 5.2 5.3 5.4 5.5 5.6 5.7 6.0 Introduction ....................................................................................................... 18 Pump Test Data Collection ............................................................................... 19 Water Level Measurements .............................................................................. 19 Pumping Rates and Volumes ............................................................................ 19 Mass Removed .................................................................................................. 20 Inspections ........................................................................................................ 20 Conditions That May Affect Water Levels in Piezometers .............................. 20 CORRECTIVE ACTION REPORT ..................................................... $0 •••••••••• 20 6.1 Assessment of Previous Quarter's Corrective Actions .......................................... 22 7.0 CONCLUSIONS AND RECOMMENDATIONS ............................................ 23 8.0 ELECTRONIC DATA FILES AND FORMAT .............................................. 25 9.0 SIGNATURE AND CERTIFICATION ........................................................... 26 LIST OF TABLES Table 1 Summary of Well Sampling for the Period Table 2 Mass of Chloroform Removed Per Well Per Quarter Table 3 Chloroform Pumping Rates and Volumes 11 N:\WMM\Required Reports\Chloroform Quarterly Monitoring Report\2012 Q3\2012_Q3Chloroform_Report_text.doc I · INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab BOrder of Sampling and Field Data Worksheets Tab C Weekly and Monthly Depth to Water Data Tab D Kriged Current Quarter Groundwater Contour Map, Capture Zone Map, Capture Zone Details Map, and Depth to Water Data Table Tab E Kriged Previous Quarter Groundwater Contour Map Tab F Hydrographs of Groundwater Elevations Over Time for Chloroform Monitoring Wells Tab G Depths to Groundwater and Elevations Over Time for Monitoring Wells Tab H Laboratory Analytical Reports Tab 1 Quality Assurance and Data Validation Tables 1 -1 Field Data QAlQC Evaluation 1-2 Holding Time Evaluation 1-3 Receipt Temperature Check 1-4 Analytical Method Check 1-5 Reporting Limit Evaluation 1 -6 Trip Blank Evaluation 1-7 QAlQC Evaluation for Sample Duplicates 1 -8 QC Control Limits for Analyses and Blanks 1-9 Rinsate Evaluation Tab J Kriged Current Quarter Chloroform Isoconcentration Map Tab K Analyte Concentration Data Over Time Tab L Chloroform Concentration Trend Graphs Tab M CSV Transmittal Letter 111 N:\ WMM\Required Reports\Chloroform Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroform _Report _text. doc 1.0 INTRODUCTION The presence of chloroform was initially identified in groundwater at the White Mesa Mill (the "Mill") as a result of split sampling performed in May 1999. The discovery resulted in the issuance of State of Utah Notice of Violation ("NOV") and Groundwater Corrective Action Order ("CAO") State of Utah Department of Environmental Quality ("UDEQ") Docket No. UGW-20-01, which required that Energy Fuels Resources (USA) Inc. ("EFRI") submit a Contamination Investigation Plan and Report pursuant to the provisions ofUAC R317-6-6.15(D). The frequency of chloroform sampling, which was initially performed on a monthly basis, was modified on November 8, 2003. Since that time all chloroform contaminant investigation wells have been sampled on a quarterly basis. This is the Quarterly Chloroform Monitoring Report for the third quarter of 2012 as required under the NOV and CAO. This Report also includes the Operations Report for the Long Term Pump Test at MW-4, TW4-19, MW-26 (previously referred to as TW4- 15), TW4-20, and TW4-4 for the quarter. 1.1 Groundwater Discharge Permit Modifications during the Quarter During the third quarter of 2012, the approved July 14, 2011 GWDP was revised on August 24, 2012. The revision incorporated the EFRI name change from Denison Mines (USA) Corp. No changes were issued to the groundwater monitoring program described herein. 2.0 CHLOROFORM MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of all groundwater monitoring wells, piezometers, existing wells, temporary chloroform contaminant investigation wells and temporary nitrate investigation wells is attached under Tab A. Chloroform samples and measurements taken during this reporting period are discussed in the remainder of this section. 2.1.1 TW 4-27 Installation of the new perched groundwater monitoring well, TW4-27, was completed on November 8, 2011, as required by the May 26, 2011 DRC Request for Additional Information ("RFI"), and as delineated in the Final EFRI Work Plan and Schedule to Drill and Install Well TW4-27 (the "Plan"), submitted to DRC on October 3,2011. Per section 1.2 of the Plan, water level and chloroform concentration data will be collected from existing wells, as well as TW4-27, to determine if TW4-27 satisfies the stipulated criteria. TW 4-27 will satisfy the stipulated criteria if the 70 ug/L chloroform isoconcentration line remains hydraulically up gradient of TW 4-27, and groundwater contour lines show that TW 4-27 is hydraulically downgradient of TW 4-4 and TW 4-6. 1 N:\ WMM\Required Reports\Chloroform Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chloroform _Report _text. doc In addition to the criteria in section 1.2, section 1.3 of the Plan states that if water level data from TW4-27 indicates that the water level at TW4-14 is anomalous, TW4-14 will be abandoned, with the approval of the Director of the Division of Radiation Control. The water level at TW4-14 will be considered anomalous if the water level at TW4-27 is comparable to the water level at TW 4-6. First and second quarter 2012 water level and analytical data collected from TW4-27 indicate that the 70 ug/L chloroform isoconcentration· line remains hydraulically upgradient of TW4-27, and that TW4-27 is hydraulically downgradient of TW4-4 and TW 4-6, satisfying the criteria described above. Furthermore, because the water level at TW4-27 is similar to the water level at TW4-14, but is approximately 14 feet lower than the water level at TW 4-6, the water level at TW 4-14 is not considered anomalous, and the section 1.3 abandonment criteria are not met. 2.1.2 Chloroform Monitoring Quarterly sampling for chloroform monitoring parameters is currently required in the following wells: TW4-1 TW4-2 TW4-3 TW4-4 TW4-5 TW4-6 TW4-7 TW4-8 TW4-9 TW4-10 TW4-11 TW4-12 TW4-13 TW4-14 TW4-16 TW4-18 TW4-19 TW4-20 TW4-21 TW4-22 TW4-23 TW4-24 TW4-25 MW-4 MW-26 (formerly TW4-15) MW -32 (formerly TW4-17) TW4-26 TW4-27 Table 1 provides an overview of all wells sampled during the quarter, along with the date samples were collected from each well, and the date(s) which analytical data were received from the contract laboratory. Table 1 also identifies equipment rinsate samples collected, as well as sample numbers associated with the deionized field blank ("DIFB") and any required duplicates. As indicated in Table 1, chloroform monitoring was performed in all of the required chloroform monitoring wells. 2.1.3 Parameters Analyzed Wells sampled during this reporting period were analyzed for the following constituents: • Chloroform • Chloromethane • Carbon tetrachloride • Methylene chloride 2 N:\WMM\Required Reports\Chlorofonn Quarterly Monitoring Report\2012 Q3\2012_ Q3Chloroform_Report_textdoc • Chloride • Nitrate plus Nitrite as Nitrogen Use of analytical methods is consistent with the requirements of the Chloroform Investigation Monitoring Quality Assurance Program (the "Chloroform QAP") attached as Appendix A to the White Mesa Uranium Mill Groundwater Monitoring QAP Revision 7.2, dated June 6, 2012. 2.1.4 Groundwater Head Monitoring Depth to groundwater was measured in the following wells andlor piezometers, pursuant to Part I.E.3 of the Groundwater Discharge Permit (the "GWDP"): • The quarterly groundwater compliance monitoring wells. • Existing monitoring well MW -4 and all of the temporary chloroform investigation wells. • Piezometers -P-1, P-2, P-3, P-4 and P-5. • MW-20 and MW-22. • ' Nitrate monitoring wells. • The DR piezometers which were installed during the Southwest Hydrologic Investigation. • In addition to the above, depth to water measurements are routinely observed in conjunction with sampling events for all wells sampled during quarterly and accelerated efforts, regardless of the sampling purpose~ In addition, weekly and monthly depth to groundwater measurements were taken in MW- 4, MW-26, TW4-19, TW4-20, and TW4-4, as part of the long term pumping test for MW-4. 2.2 Sampling Methodology and Equipment and Decontamination Procedures EFRI completed, and transmitted to UDEQ on May 25, 2006, a revised QAP for sampling under the Mill's Groundwater Discharge Permit ("GWDP"). While the water sampling conducted for chloroform investigation purposes has conformed to the general principles set out in the QAP, some of the requirements in the QAP were not fully implemented prior to UDEQ's approval, for reasons set out in correspondence to UDEQ dated December 8, 2006. Subsequent to the delivery of the December 8, 2006 letter, EFRI discussed the issues brought forward in the letter with UDEQ and has received correspondence from UDEQ about those issues. In response to UDEQ's letter and subsequent discussions with UDEQ, EFRI has incorporated changes in chloroform Quality Assurance ("QA") procedures in the form of the Chloroform QAP. The Chloroform QAP describes the needs of the chloroform investigation program where they differ from the Groundwater QAP. On June 20, 2009 the Chloroform QAP was modified to require that the quarterly chloroform reports include additional items specific to EFRI's ongoing pump testing and chloroform capture efforts. The Groundwater QAP as well as the Chloroform QAP were revised again on June 7, 2012. The revised 3 N:\WMM\Required Reports\Chloroform Quarterly Monitoring Report\2012 Q3\2012_ Q3Chloroform_Report_text.doc Groundwater QAP and Chloroform QAP, Revision 7.2 were approved by DRC on June 7, 2012. The sampling methodology, equipment and decontamination procedures that were used for the chloroform contaminant investigation, as summarized below, are consistent with the newly approved QAP Revision 7.2 and the Chloroform QAP. 2.2.1 Well Purging and Depth to Groundwater A list of the wells in order of increasing chloroform contamination is generated quarterly. The order for purging is thus established., __ The list is included with the Field Data Worksheets under Tab B. Mill personnel start purging with all of the non-detect wells and then move to the more contaminated wells in order of chloroform contamination. Samples are collected by means of disposable bailer(s) the day following the purging. The disposable bailer is used only for the collection of a sample from an individual well and disposed subsequent to the sampling. The wells are purged prior to sampling by means of a portable pump. Each quarterly purging event begins at the location least affected by chloroform (based on the previous quarters sampling event) and proceeds by affected concentration to the most affected location. As noted in the approved QAP, Revision 7.2, purging will generally follow this order, and the sampling order may deviate slightly from the generated list. This practice does not affect the samples for these reasons: any wells sampled in slightly different order have either dedicated pumps or are sampled via a disposable bailer. This practice does not affect the quality or usability of the data as there will be no cross-contamination resulting from sampling order. Before leaving the Mill office, the portable pump and hose are rinsed with deionized ("DI") water. Where portable (non-dedicated) sampling equipment is used, a rinsate sample will be collected at a frequency of one rinsate sample per 20 field samples. Well depth measurements are taken and the one casing volume is calculated for those wells which do not have a dedicated pump as described in Attachment 2-3 of the QAP. Purging is completed to remove stagnant water from the casing and to assure that representative samples of formation water are collected for analysis. There are three purging strategies that will be used to remove stagnant water from the casing during groundwater sampling at the Mill. The three strategies are as follows: 1. Purging three well casing volumes with a single measurement of field parameters specific conductivity, turbidity, pH, redox potential, and water temperature 2. Purging two casing volumes with stable field parameters for specific conductivity, turbidity, pH, redox potential, and water temperature (within 10% RPD) 3. Purging a well to dryness and stability of field parameters for pH, specific conductivity, and water temperature only after recovery If the well has a dedicated pump, it is pumped on a set schedule per the remediation plan and is considered sufficiently evacuated to immediately collect a sample; however, if a pumping well has been out of service for 48 hours or more, EFRI will follow the purging requirements outlined in Attachment 2-3 of the QAP. The dedicated pump is used to 4 N:\WMM\Required Reports\Chloroform Quarterly Monitoring Report\2012 Q3\20 12_ Q3Chioroform _Report_text. doc collect parameters and to collect the samples as described below. If the well does not have a dedicated pump, a Grundfos pump (9 -10 gpm pump) is then lowered to the screened interval in the well and purging is started. The purge rate is measured for the well by using a calibrated 5 gallon bucket. This purging process is repeated at each well location moving from least contaminated to the most contaminated well. All wells are capped and secured prior to leaving the sampling location. Wells with dedicated pumps are sampled when the pump is in the pumping mode. If the pump is not pumping at the time of sampling, it is manually switched on by the Mill Personnel. The well is pumped for approximately 5 to 10 minutes prior to the collection of the field parameters. Per the approved QAP, one set of parameters is collected. Samples are collected following the measurement of one set of field parameters. The pump is turned off and allowed to resume its timed schedule. 2.2.2 Sample Collection Samples are collected as described above. In all cases, on days when samples will be collected, a cooler with ice is prepared. The trip blank is also gathered at that time (the trip blank for these events is provided by the Analytical Laboratory). Once Mill Personnel arrive at the well sites, labels are filled out for the various samples to be collected. All personnel involved with the collection of water and samples are then outfitted with rubber gloves. Chloroform investigation samples are collected by means of disposable bailers. Mill personnel use a disposable bailer to sample each well that does not have a dedicated pump. The bailer is attached to a reel of approximately 150 feet of nylon rope and then lowered into the well. After coming into contact with the water, the bailer is allowed to sink into the water in order to fill. Once full, the bailer is reeled up out of the well and the sample bottles are filled as follows: • Volatile Organic Compound ("VOC") samples are collected first. This sample consists of three 40 ml vials provided by the Analytical Laboratory. The VOC sample is not filtered and is preserved with HCI; • A sample for nitrate/nitrite is then collected. This sample consists of one 250 ml. bottle which is provided by the Analytical Laboratory. The nitrate/nitrite sample is also not filtered and is preserved with H2S04; • A sample for chloride is then collected. This sample consists of one 500 ml. bottle which is provided by the Analytical Laboratory. The chloride sample is also not filtered and is not chemically preserved. After the samples have been collected for a particular well, the bailer is disposed of and the samples are placed into the cooler that contains ice. The well is then recapped and Mill personnel proceed to the next well. 5 N:\ WMM\Required Reports\Chloroform Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroform _Report _text. doc 2.3 Field Data Attached under Tab B are copies of all Field Data Worksheets that were completed during the quarter for the chloroform contaminant investigation monitoring wells identified in paragraph 2.1.1 above, and Table 1. 2.4 Depth to Groundwater Data and Water Table Contour Map Attached under Tab C are copies of the Depth to Water Sheets for the weekly monitoring of MW-4, MW-26, TW4-19, TW4-20, and TW4-4, as well as the monthly depth to groundwater data for chloroform contaminant investigation wells measured during the quarter. Depth to groundwater measurements which were utilized for groundwater contours are included on the Quarterly Depth to Water Worksheet at Tab D of this report, along with the kriged groundwater contour map for the current quarter generated from this data. A copy of the kriged groundwater contour map generated from the previous quarter's data is provided under Tab E. 2.5 Laboratory Results 2.5.1 Copy of Laboratory Results All analytical results were provided by Energy Laboratories ("EL"). Table 1 lists the dates when analytical results were reported to the QA Manager for each sample. Results from analysis of samples collected for this quarter's chloroform contaminant investigation are provided under Tab H of this Report. Also included under Tab Hare the results of analyses for duplicate samples, the DIFB, and rinsate samples for this sampling effort, as identified in Table 1, as well as results for trip blank analyses required by the Chloroform QAP. 2.5.2 Regulatory Framework As discussed in Section 1.0, above, the NOV and requirements of the CAO triggered a series of actions on EFRI's part. In addition to the monitoring program, EFRI has equipped five wells with pumps to recover impacted groundwater, and has initiated recovery of chloroform from the perched zone. Sections 4 and 5, below, interpret the groundwater level and flow information, contaminant analytical results, and pump test data to assess effectiveness of EFRI's chloroform capture program. 3.0 QUALITY ASSURANCE AND DATA VALIDATION The QA Manager performed a QAlQuality Control ("QC") review to confirm compliance of the monitoring program with requirements of the QAP. As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and QC review of laboratory methods and data. Identification of field QC samples collected and analyzed is provided in Section 6 N:\WMM\Required Reports\Chloroform Quarterly Monitoring Report\2012 Q3\2012_ Q3 Chloroform_Report_text. doc 3.1. Discussion of adherence to Mill sampling Standard Operating Procedures ("SOPs") is provided in Section 3.2. Analytical completeness review results are provided in Section 3.3. The steps and tests applied to check laboratory data QAlQC are discussed in Sections 3.4.4 through 3.4.9 below. The analytical laboratory has provided summary reports of the analytical QAlQC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference ("NELAC") certification and reporting protocol. The Analytical Laboratory QAlQC Summary Reports, including copies of the Mill's Chain of Custody and Analytical Request Record forms for each set of Analytical Results, follow the analytical results under Tab H. Results of review of the laboratory QAlQC information are provided under Tab I and are discussed in Section 3.4, below. 3.1 Field QC Samples The following QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program. Field QC samples for the chloroform investigation program consist of one field duplicate sample for each 20 samples, a trip blank for each shipped cooler which contains VOCs, one DIFB and rinsate samples. During this quarter, two duplicate samples were collected as indicated in Table 1. The duplicates were sent blind to the analytical laboratory and analyzed for the same parameters as the chloroform wells. Three trip blanks were provided by Energy Laboratories and returned with the quarterly chloroform monitoring samples. Two rinsate blank samples were collected at a frequency of one rinsate per twenty samples per QAP Section 4.3.2 and as indicated on Table 1. Rinsate samples were labeled with the name of the subsequently purged well with a terminal letter "R" added (e.g. TW 4-7R). The results of these analyses are included with the routine analyses under TabH. In addition, one DIFB, while not required by the Chloroform QAP, was collected and analyzed for the same constituents as the well samples and rinsate blank samples. 3.2 Adherence to Mill Sampling SOPs On a review of adherence by Mill personnel to the existing sampling SOPs, the QA Manager observed that QAlQC requirements established in the QAP and Chloroform QAP were being adhered to. 7 N:\ WMM\Required Reports\Chloroform Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroform _Report _text. doc 3.3 Analyte Completeness Review All analyses required by the CAO for chloroform monitoring for the period were performed. 3.4 Data Validation The QAP and GWDP identify the data validation steps and data QC checks required for the chloroform monitoring program. Consistent with these requirements, the QA Manager performed the following evaluations: a field data QAlQC evaluation, a holding time check, a receipt temperature check, an analytical method check, a reporting limit evaluation, a trip blank check, a QAlQC evaluation of sample duplicates, a QC Control Limit check for analyses and blanks including the DIFB and a rinsate sample check. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab I. 3.4.1 Field Data QAlQC Evaluation The QA Manager performs a review of all field recorded parameters to assess their adherence with QAP requirements. The assessment involved review of two sources of information: the Field Data Sheets and the Quarterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and measurement of field parameters based on the requirements discussed in section 2.2.1 above. The purging technique employed determines the requirements for field parameter measurement and whether stability criteria are applied. Review of the Depth to Water data confirms that all depth measurements used for development of groundwater contour maps were conducted within a five-day period as indicated by the measurement dates in the summary sheet under Tab D. The results of this quarter's review offield data are provided under Tab I. Based upon the review of the field data sheets, all wells conformed to the QAP purging and field measurement requirements. A summary of the purging techniques employed and field measurements taken is described below: Purging Two Casing Volumes with Stable Field Parameters (within 10% RPD) Wells TW4-01, TW4-05, TW4-08, TW4-09, TW4-11, TW4-12, TW4-16, MW-32, TW4- 21, TW4-23, TW4.,.24, and TW4-25 were sampled after two casing volumes were removed. Field parameters pH, specific conductivity, turbidity, water temperature, and redox potential were measured during purging. All field parameters for this requirement were stable within 10% RPD. Purging a Well to Dryness and Stability of a Limited List of Field Parameters Wells TW4-2, TW4-3, TW4-6, TW4-7, TW4-10, TW4-13, TW4-14, TW4-22, TW4-26, and TW4-27 were pumped to dryness before two casing volumes were evacuated. After well recovery, one set of measurements for the field parameters of pH, specific conductivity, and water temperature only were taken, the samples were collected, and another set of measurements for pH, specific conductivity, and water temperature were taken. Stabilization of pH, conductivity and temperature are required within 10% RPD under the QAP, Revision 7.2. It is important to note that redox potential and turbidity 8 N:\ WMM\Required Reports\Chloroform Quarterly Monitoring Report\2012 Q3\2012 _ Q3Chioroform _ Report_text. doc were measured as well during purging and sampling. These parameters were not within 10% RPD; however, these parameters are not required to be measured or to be within 10% RPD per the approved QAP, Revision 7.2. Data from measurement of these parameters has been provided for information purposes only. During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water to the nearest 0.01 foot. The revie\-v of the field sheets for compliance with QAP, Revision 7.2 requirements resulted in the observations noted below. The QAP requirements in Attachment 2-3 specifically state that field parameters must be stabilized to within 10% over at least 2 consecutive measurements. The QAP Attachment 2-3 states that turbidity should be less than 5 NTU prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP Attachment 2-3 does not require that turbidity measurements be less than 5 NTU prior to sampling. As such the noted observations regarding turbidity measurements greater than 5 NTU below are included for information purposes only. Wells TW4-01, TW4-02, TW4-05, TW4-06, TW4-07, TW4-08, TW4-09, TW4-10, TW4-11, TW4-12, TW4-16, MW-32, TW4-18, TW4-21, TW4-23, TW4-24, TW4-25, TW4-26, and TW4-27 exceeded the QAP's 5 NTU goal. The QAP does not require that turbidity measurements be less than 5 NTU prior to sampling. Of the nineteen samples, six samples (TW4-02, TW4-06, TW4-07, TW4-10, TW4-26, and TW4-27) were taken after the well had been pumped to dryness. In wells that are purged to dryness, turbidity is not required per the QAP, Revision 7.2. As such, the noted observations regarding turbidity measurements less than 5 NTU are included for information purposes only. EFRI's letter to DRC of March 26,2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In response to DRC's subsequent correspondence dated June 1, 2010 and June 24, 2010, EFRI has completed a monitoring well redevelopment program. The redevelopment report was submitted to DRC on September 30, 2011. DRC responded to the redevelopment report via letter on November 15, 2012. Per the DRC letter dated November 15, 2012, the field data generated this quarter are compliant with the turbidity requirements of the approved QAP. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided in Tab I. The Trip Blank sample collected on 9110/2012 was analyzed by the laboratory outside of the required holding time. The samples were received at the lab on 9/14/2012, but were not analyzed until 9/26/2012. All other samples received by the laboratory with the Trip Blank were analyzed within required holding time. EFRI Field Personnel shipped the samples, and they were received by the laboratory with more than sufficient time to analyze the samples within required holding time. This is due to a laboratory error and did not result from any actions or inactions EFRI. Not only was EFRI not informed of the missed holding time by the laboratory, the original data p'ackage sent from the laboratory did not flag the sample as being outside required holding time. It was not until EFRI's manual QAlQC evaluation 9 N:\ WMM\Required Reports\Chlorofonn Quarterly Monitoring Report\20 12 Q3\20 12_ Q3 Chloroform_Report _text. doc that the issue was identified. Corrective actions for this issue are described in Section 6.1. 3.4.3 Receipt Temperature Evaluation Chain of Custody sheets were reviewed to confirm compliance with the QAP requirement which specifies that samples be received at 6°C or lower. Sample temperatures checks are provided in Tab I. All samples were received within the required temperature limit. 3.4.4 Analytical Method Checklist All analytical methods reported by the laboratory were checked against the required methods enumerated in the Chloroform QAP. Analytical method checks are provided in Tab I. All methods were consistent with the requirements of the Chloroform QAP. 3.4.5 Reporting Limit Evaluation All analytical method reporting limits reported by the laboratory were checked against the reporting limits enumerated in the Chloroform QAP. Reporting Limit Checks are provided under Tab I. All analytes were measured and reported to the required reporting limits, except 30 sets (28 samples and 2 duplicates) of sample results had the reporting limit raised for at least one analyte due to matrix interference and/or sample dilution. In all cases the reported value for the analyte was higher than the increased detection limit. 3.4.6 Receipt pH Evaluation Appendix A of the QAP states that all volatile samples are required to be preserved and arrive at the laboratory with a pH less than 2. A review of the laboratory data revealed that all volatile samples were received at the laboratory with a pH less than 2 except for one, TW4-24. In past cases where a sample was outside of acceptable pH limits, the laboratory notified EFRI at the time of analysis so that a new sample could be collected; however in this case, EFRI was not informed of the issue by the laboratory at the time of analysis. The sample was not recollected, because EFRI became aware of the issue after the end of the third quarter. The laboratory noted the pH of the sample from TW 4-24 was 5 at the time of analysis. This would indicate that the sample was not preserved. Per EPA SW-846 Chapter 4, Organic Analytes, Section 4.1.2, the standard holding time for a preserved VOC sample is 14 days, and the standard holding time for a non-preserved VOC sample is 7 days. The analysis was completed by the laboratory within 7 days per the EPA standard for a non- preserved sample, rather than the 14 days as required by the QAP. Since the sample was analyzed within EPA required hold time for non-preserved samples, the data are useable and not rej ected. " Corrective actions for this issue are described in Section 6.1. 10 N:\ WMM\Required Reports\Chlorofonn Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroform _Report _text. doc 3.4.7 Trip Blank Evaluation All trip blank results were reviewed to identify any VOC contamination resulting from transport of the samples. Trip blank checks are provided in Tab 1. All trip blank results were less than the reporting limit for all VOCs. 3.4.8 QAlQC Evaluation for Sample Duplicates Section 9.1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results are less than 5 times the required detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for all duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits; however, data will be considered noncompliant only when the results are greater than 5 times the reported detection limit and the RPD is greater than 20%. The additional duplicate information is provided for information purposes. All analytical results for the sample/duplicate pairs were within the 20% acceptance limits except one. The chloroform result for the parent sample, TW4-25, was non-detect, while the duplicate sample, TW 4-70, result was 1.3 ug/L resulting in an RPD greater the 20%. However, per section 9.1.4 a) of the QAP, sample duplicates will be considered noncompliant only when the results are greater than 5 times the required reporting limit and the RPD is greater than 20%. The sample/duplicate results in this case are not greater than 5 times the reporting limit and therefore are considered acceptable. All results of the RPD test are provided in Tab 1. 3.4.9 Rinsate Sample Check Rinsate blank sample checks are provided in Tab 1. A comparison of the rinsate blank sample concentration levels to the QAP requirements -that rinsate sample concentrations be one order of magnitude lower than that of the actual well -indicated that all of the rinsate blank analytes met this criterion. While not required by the Chloroform QAP, DIFB samples are collected to analyze the quality of the DI water system at the Mill, which is also used to collect rinsate samples. A review of the analytical results reported for the DIFB sample indicated the sample contained chloroform. Further review of the data package showed that the DIFB sample was analyzed by the lab immediately after the samples with the highest levels of chloroform. As the rinsates collected for the quarter are non-detect, EFRI believes the chloroform present in the DIFB is due to carry-over at the lab and does not represent actual chloroform contamination in the DI water system at the Mill. No formal corrective action will be provided, however, EFRI is planning to change laboratories for the first Quarter 2013 sampling event. 11 N:\ WMM\Required Reports\Chloroform Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroform _Report _text. doc 3.4.10 Other Laboratory QAlQC Section 9.2 of the QAP requires that the laboratory's QAlQC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate analytical laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, EFRI's QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specified acceptance limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided in Tab I. All lab QAlQC results met these specified acceptance limits except as noted below. The QAP Section 8.1.2 requires that a Matrix Spike/Matrix Spike Duplicate ("MS/MSD") pair be analyzed with each analytical batch. The QAP does not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the MS/MSD pair be prepared on EFRI samples only. Acceptance limits for MS/MSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the QAP requirement to analyze an MS/MSD pair with each analytical batch was met. While the QAP does not require it, the recoveries were reviewed for compliance with the laboratory established acceptance limits. The QAP does not require this level of review, and the results of this review are provided for information only. The information from the Laboratory QAlQC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for all quarterly chloroform samples are within acceptable laboratory limits for all regulated compounds except as indicated in Tab I. One MS/MSD recovery RPD was are outside the laboratory established acceptance limits. This result does not affect the quality or usability of the data because the recoveries and RPDs above or below the acceptance limits are indicative of matrix interference. Fourteen MS/MSD recoveries were above the laboratory established acceptance limits, indicating a high bias to the individual sample results. A high bias means that reported results may be higher than the actual results. One MS/MSD recovery was below the laboratory established acceptance limits. The lab noted on this MS/MSD that the target compound matrix carryover from previous samples caused interference for the chloroform recoveries. The recoveries do not affect the quality or usability of the data because the recoveries outside of the acceptance limits are indicative of matrix interference. The QAP requirement to analyze a MS/MSD pair with each analytical batch was met and as such the data are compliant with the QAP. The QAP specifies that surrogate compounds shall be employed for all organic analyses, but the QAP does not specify acceptance limits for surrogate recoveries. The analytical data associated with the routine quarterly sampling met the requirement specified in the QAP. The information from the Laboratory QAlQC Summary Reports indicates that the 12 N:\WMM\Required Reports\Chlorofonn Quarterly Monitoring Report\2012 Q3\2012_Q3Chloroform_Report_text.doc surrogate recoveries for all quarterly chloroform samples were within acceptable laboratory limits for all surrogate compounds except as indicated in Tab 1. One hundred and one surrogate recoveries were above the laboratory established acceptance limits, indicating a high bias to the individual sample results. A high bias means that reported results may be higher than the actual results. One surrogate recovery was below the laboratory established acceptance limits. The surrogate compounds outside of acceptance limits are most likely the result of laboratory spiking compound degradation. This is apparent because the same compounds were outside the compliance limits in all samples analyzed within a specific period of time. There is no effect on the quality or usability of the data, because the low surrogate recoveries were on a laboratory matrix spike which would indicate surrogate solution degradation at the laboratory. These recoveries do not impact other results, because there are multiple surrogates added to each sample and all other surrogates were within limits. Furthermore, there are no QAP requirements for surrogate recoveries. The information from the Laboratory QAlQC Summary Reports indicates that all LCS recoveries were within acceptable laboratory limits for all LCS compounds except as indicated in Tab 1. There were five LCS recoveries which were above the laboratory established acceptance limits, and as such indicate a high bias to the sample results associated with that LCS. It is important to note that there is no requirement in the QAPs for LCS recovery assessment. 4.0 INTERPRETATION OF DATA 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions. 4.1.1 Current Site Groundwater Contour Map As stated above, a listing of groundwater level readings for the current quarter (shown as depth to groundwater in feet) is included under Tab D. The data from this tab has been interpreted (kriged) and plotted in a water table contour map, provided under the same tab. Also included under Tab D is a groundwater contour map of the Mill site and a more detailed map of a portion of the Mill site where the chloroform pumping wells are located, in each case with hand-drawn stream tubes, depicting hydraulic capture from the pumpIng. The water level contour maps indicate that perched water flow ranges from generally southwesterly beneath the Mill site and tailings cells to generally southerly along the eastern and western margins of White Mesa. Perched water mounding associated with the wildlife ponds locally changes the flow patterns. For example, northeast of the Mill site, mounding associated with wildlife ponds results in locally northerly flow near MW -19. The impact of the water level mound associated with the northern ponds, which are no longer receiving water, is diminishing and is expected to continue to diminish in the future as the water level mound decays due to reduced recharge. Flow directions are also locally influenced by pumping at MW-4, MW-26, TW4-4, TW4-19, and TW4-20. 13 N:\WMM\Required Reports\Chlorofonn Quarterly Monitoring Report\2012 Q3\2012_ Q3Chloroformyeport_text.doc Significant cones of depression have formed in the vicinity of all pumping wells except TW4-4, which began pumping in the first quarter of2010. Although pumping at TW4-4 has depressed the water table in the vicinity of TW4-4, a well-defined cone of depression is not evident. The lack of a well-defined cone of depression likely results from 1) variable permeability conditions in the vicinity of TW 4- 4, and 2) persistent relatively low water levels at adjacent well TW 4-14. Changes in water levels at wells immediately south of TW 4-4 resulting from TW 4-4 pumping are expected to be muted because TW 4-4 is located at a transition from relatively high to relatively low permeability conditions south (downgradient) of TW4-4. The permeability of the perched zone at TW4-6 and TW4-26 is approximately two orders of magnitude lower than at TW 4-4. Any drawdown of water levels at wells immediately south of TW 4-4 resulting from TW 4-4 pumping is also difficult to determine because of a general, long-term increase in water levels in this area. Water levels at TW4-4 and TW4- 6 increased by nearly 2.7 and 2.9 feet, respectively, between the fourth quarter of 2007 and the fourth quarter of 2009 Gust prior to TW 4-4 pumping) at rates of approximately 1.2 feet/year and 1.3 feet/year, respectively. However, the increase in water level at TW4- 6 has been reduced since the start of pumping at TW 4-4 (first quarter of 2010) to less than 0.5 feet/year suggesting that TW4-6 is within the hydraulic influence of TW4-4. The lack of a well-defined cone of depression at TW 4-4 is also influenced by the persistent, relatively low water level at non-pumping well TW 4-14, located east of TW 4- 4 and TW4-6. For the current quarter, the water level at TW4-14 (approximately 5526 feet above mean sea level [ft amsl]) is approximately 13 feet lower than the water level at TW4-6 (approximately 5539 ft amsl) and approximately 17 feet lower than at TW4-4 (approximately 5543 ft amsl) even though TW4-4 is pumping. Well TW4-27 (installed south of TW4-14 in the fourth quarter of2011) has a static water level of approximately 5526 ft amsl, similar to TW4-14. TW4-27 was positioned at a location considered likely to detect any chloroform present and/or to bound the chloroform plume to the southeast and east of TW 4-4 and TW 4-6. As will be discussed below, groundwater data collected since installation indicates that TW4-27 does indeed bound the chloroform plume to the southeast and east of TW 4-4 and TW 4-6. Prior to the installation of TW4-27, the persistently low water level at TW4-14 was considered anomalous because it appeared to be downgradient of all three wells TW4-4, TW4-6, and TW4-26, yet chloroform was not detected at TW4-14. Chloroform had apparently migrated from TW4-4 to TW4-6 and from TW4-6 to TW4-26 which suggested that TW 4-26 was actually downgradient of TW 4-6, and TW 4-6 was actually downgradient of TW 4-4, regardless of the flow direction implied by the low water level at TW4-14. The water level at TW4-26 (5538.6 feet amsl) is, however, lower than water levels at adjacent wells TW4-6 (5539.0 feet amsl), and TW4-23 (5542.9 feet amsl) Hydraulic tests conducted in November, 2011 indicate that the permeability at TW4-27 is an order of magnitude lower than at TW 4-6 and three orders of magnitude lower than at TW4-4. The similar water levels at TW4-14 and TW4-27, and the low permeability estimate at TW4-27 suggest that both wells are completed in materials having lower 14 N:\WMM\Required Reports\Chlorofonn Quarterly Monitoring Report\2012 Q3\2012_ Q3Chloroform_Report_text.doc permeability than nearby wells. The low permeability condition likely reduces the rate of long-term water level increase at TW4-14 and TW4-27 compared to nearby wells, yielding water levels that appear anomalously low. The low permeability condition is expected to retard the transport of chloroform to TW4-14 and TW4-27 (compared to nearby wells). As will be discussed in Section 4.2.3, third quarter, 2012 chloroform concentrations at TW 4-26 and TW 4-27 are 6.9 ug/L and non-detect, respectively and both wells are outside the chloroform plume. 4.1.2 Comparison of Current Groundwater Contour Maps to Groundwater Contour Maps for Previous Quarter The groundwater contour maps for the Mill site for the second quarter of 2012, as submitted with the Chloroform Monitoring Report for the second quarter of 2012, are attached under Tab E. A comparison of the water table contour maps for the current (third) quarter of 2012 to the water table contour maps for the previous quarter (second quarter of 2012) indicates similar patterns of drawdown related to pumping of MW -4, MW -26, TW 4-4, TW 4-19 and TW4-20. Water levels and water level contours for the site have not changed significantly since the last quarter, except for a few locations. As discussed in Section 4.1.1, pumping at TW4-4, which began in the first quarter of 2010, has depressed the water table near TW4-4, but a well-defined cone of depression is not yet evident, likely due to variable permeability conditions near TW 4-4 and the persistently low water level at adjacent well TW4-14. Reported increases in water level of approximately 3 feet occurred in well MW-20 and of approximately 6 feet occurred in well TW 4-12, and decreases of approximately 6 feet occurred in PIEZ-2, and of approximately 3 feet occurred in TWN-2. The water level change at PIEZ-2 is consistent with the cessation of water delivery to the northern wildlife ponds. The water level changes at other non-pumping wells were less than 3 feet. A water level decrease (increase in drawdo~) of nearly 7 feet occurred in pumping well MW-26. Water level fluctuations at pumping wells MW-4, MW-26, TW4-4, TW4-19, and TW4- 20 typically occur in part because of fluctuations in pumping conditions just prior to and at the time the measurements are taken. Water levels reported at all pumping wells other than MW-26 this quarter were within 2 feet of their reported water levels last quarter. 4.1.3 Hydrographs Attached under Tab Fare hydro graphs showing groundwater elevation In each chloroform contaminant investigation monitor well over time. 4.1.4 Depth to Groundwater Measured and Groundwater Elevation Attached under Tab G are tables showing depth to groundwater rneasured and groundwater elevation over time for each of the wells listed in Section 2.1.1 above. 15 N:\WMM\Required Reports\Chlorofonn Quarterly Monitoring Report\2012 Q3\20 12_ Q3Chioroform _Report _text. doc "- 4.1.5 Evaluation of the Effectiveness of Hydraulic Capture Perched water containing chloroform has been removed from the subsurface by pumping MW-4, MW-26, TW4-4, TW4-19, and TW4-20. The primary purpose of the pumping is to reduce total chloroform mass in the perched zone as rapidly as is practical. Wells upgradient of TW 4-4 were chosen for pumping because 1) they are located in areas of the perched zone having relatively high permeability and saturated thickness, and 2) high concentrations of chloroform were detected at these locations. The relatively high transmissivity of the perched zone in the vicinity of these pumping wells results in the wells having a relatively high productivity. The combination of relatively high productivity and high chloroform concentrations allows a high rate of chloroform mass removal. TW 4-4 is located in a downgradient area having relatively high chloroform concentrations but relatively small saturated thickness, and at a transition from relatively high to relatively low permeability conditions downgradient of TW 4-4. As with the other pumping wells, pumping TW 4-4 helps to reduce the rate of chloroform migration in downgradient portions of the plume. The impact of pumping is indicated by the water level contour maps attached under Tabs D and E. Cones of depression have developed in the· vicinity of MW -4, MW -26, TW 4- 19, and TW4-20 which continue to remove significant quantities of chloroform from the perched zone. The water level contour maps indicate effective capture of water containing high chloroform concentrations in the vicinities of these pumping wells. Overall, the combined capture of MW-4, MW-26, TW4-19, and TW4-20 has not changed significantly since the last quarter. As discussed in Section 4.1.1, the drawdown associated with TW 4-4 is likely less apparent due to variable permeability conditions near TW4-4 and the persistently low water level at adjacent well TW4-14. Chloroform concentrations exceeding 70 ~g/L have occurred in the past at some locations downgradient of pumping wells (for example, at TW4-6, located immediately south of TW4-4), where the lower permeability and relatively small saturated thickness of the perched zone significantly limits the rate at which chloroform mass can be removed by pumping. By removing mass and reducing hydraulic gradients, thereby reducing the rate of downgradient chloroform migration, and allowing natural attenuation to be more effective, pumping at the productive, up gradient locations has a beneficial effect on this downgradient chloroform. Pumping at TW 4-4 was implemented during the first quarter of 2010 to improve capture in this downgradient area to the extent allowable by the lower productivity conditions presumed to exist in this area. The beneficial effect of pumping TW 4-4 is demonstrated by the decrease in chloroform concentrations at TW4-6 from 1000 ~g/L to 6.9 ~g/L, and at TW4-26 from 13 ~g/L to 4.9 ~g/L since pumping began at TW 4-4. Concentrations at these wells have decreased substantially even though they do not unambiguously appear to be within the hydraulic capture of TW 4-4. As discussed in Section 4.1.1, however, the decrease in the long-term rate of water level rise at TW 4-6 since pumping began at TW 4-4 does suggest that TW 4-6 is within the hydraulic influence of TW4-4. Regardless of whether TW4-6 can be demonstrated to be within hydraulic capture of TW 4-4, pumping TW 4-4 reduces chloroform migration to TW 4-6 and TW 4-26 by the mechanisms discussed above. 16 N:\WMM\Required Reports\Chloroform Quarterly Monitoring Report\2012 Q3\20 12_ Q3Chloroform _ Report_text.doc 4.2 Review of Analytical Results 4.2.1 Current Chloroform Isoconcentration Map Included under Tab J of this Report is a current chloroform isoconcentration map for the Mill site. 4.2.2 Chloroform Concentration Trend Data and Graphs Attached under Tab K are tables summarizing values for all required parameters, chloride, nitrate/nitrite, carbon tetrachloride, chloroform, chloromethane, and methylene chloride, for each well over time. Attached under Tab L are graphs showing chloroform concentration trends in each monitor well over time. 4.2.3 Interpretation of Analytical Data Comparing the analytical results to those of the previous quarter, as summarized in the table included under Tab K, the following observations can be made: a) Chloroform concentrations have increased by more than 20% in the following wells compared to last quarter: MW-26, TW4-S, TW4-6, TW4-10, TW4-18, TW4-19 and TW4-22; b) Chloroform concentrations have decreased by more than 20% in the following well compared to last quarter: TW4-20; c) Chloroform concentrations have remained within 20% in the following wells compared to last quarter: MW-4, TW4-1, TW4-2, TW4-4, TW4-7, TW4-11, TW 4-21, and TW 4-26; d) MW-32, TW4-3, TW4-8, TW4-9, TW4-12, TW4-13, TW4-14, TW4-16, TW4- 23, TW4-2S and TW4-27 remained non-detect; and e) Chloroform concentrations at TW 4-24 increased from non-detect to 1.1 ~g/L. As indicated, chloroform concentrations at many of the wells with detected chloroform were within 20% of the values reported for the wells during the previous quarter, suggesting that variations are within the range typical for sampling and analytical error. Wells MW-26, TW4-S, TW4-6, TW4-10, TW4-18, TW4-19, TW4-20, and TW4-22 had changes in concentration greater than 20%. Of the latter, MW-26, TW4-19, and TW4-20 are pumping wells. TW4-7 is located adjacent to pumping well MW-4; TW4-10 is located adjacent to pumping well MW-26; TW4-S and TW4-22 are located adjacent to pumping well TW4-20; TW4-18 is located adjacent to pumping well TW4-19; and TW4- 6 is located adjacent to pumping well TW4-4. Fluctuations in concentrations at pumping wells and wells adjacent to pumping wells likely result in part from changes in pumping. 17 N:\WMM\Required Reports\Chloroform Quarterly Monitoring Report\2012 Q3\20 12_ Q3Chloroform _ Report_text.doc Pumping well TW 4-20 had the highest detected chloroform concentration. Since the last quarter, the chloroform concentration in TW4-20 decreased from 36,000 J,!g/L to 13,000 J,!g/L, the concentration in adjacent pumping well TW4-19 increased from 460 J,!g/L to 950 J,!g/L, the concentration in nearby well TW4-21 increased slightly from 400 to 410 J,!g/L, and the concentration in nearby well TW4-22 increased from 120 J,!g/L to 940 J,!g/L. Wells TW4-23 and TW4-25 remained non-detect for chloroform. The concentration in well TW 4-24 increased from non-detect to 1.1 J,!g/L. TW 4-24, located west of TW4-22, and TW4-25, located north of TW4-21 , bound the chloroform plume to the west and north. In addition, the southernmost boundary of the plume remains between TW 4-4 and TW 4-6 (located just north of southernmost temporary well TW 4-26). The chloroform concentration in TW4-6 increased from 4.7 J,!g/L to 6.9 J,!g/L, and remains outside the chloroform plume boundary. Concentrations at TW4-6 have, since initiation of pumping of TW 4-4 in the first quarter of 2010, decreased from 1000 J,!g/L to 6.9 J,!g/L. TW 4-6, installed in the second quarter of 2000, was the most downgradient temporary perched well prior to installation of temporary well TW4-23 in 2007 and temporary well TW4-26 in the second quarter of 2010. TW4-6 remained outside the chloroform plume between the second quarter of 2000 and the fourth quarter of 2008. TW 4-6 likely remained outside the chloroform plume during this time due to a combination of 1) slow rates of downgradient chloroform migration in this area due to low permeability conditions and the effects of upgradient chloroform removal by pumping, and 2) natural attenuation. Because TW 4-6 is again outside the plume boundary, TW4-6 and TW4-23 bound the chloroform plume to the south. TW4-8, TW4- 12, TW4-13, TW4-14, and TW4-27 bound the chloroform plume to the east. The slow rate of chloroform migration in the vicinity of TW 4-6 is demonstrated by comparing the rate of increase in chloroform at this well to the rate of increase in the nearest upgradient well TW 4-4. Concentrations at TW 4-4 increased from non-detect to more than 2,200 J,!g/L within only 2 quarters whereas 16 quarters were required for concentrations in TW 4-6 to increase from non-detect to only 81 J,!g/L. This behavior is consistent with hydraulic tests performed at TW4-4, TW4-6, and TW4-26 during the third quarter of 2010 that indicate a nearly two order of magnitude decrease in permeability downgradient of TW 4-4. Chloroform migration rates in the vicinity of well TW4-26 and new well TW4-27 are also expected to be relatively low due to upgradient pumping and low permeability conditions. 5.0 LONG TERM PUMP TEST AT MW-4, MW-26, TW4-19, TW4-20, AND TW4-4 OPERATIONS REPORT 5.1 Introduction As a part of the investigation of chloroform contamination at the Mill site, EFRI has been conducting a Long Term Pump Test on MW-4, TW4-19, MW-26, and TW4-20, and, since January 31, 2010, TW4-4. The purpose of the test is to serve as an interim action that will remove a significant amount of chloroform-contaminated water while gathering additional data on hydraulic properties in the area of investigation. The following information documents the operational activities during the quarter. 18 N:\WMM\Required Reports\Chloroform Quarterly Monitoring Report\2012 Q3\2012_ Q3Chloroform_Report_text.doc 5.2 Pump Test Data Collection The long term pump test for MW-4 was started on April 14, 2003, followed by the start of pumping from TW4-19 on April 30, 2003, from MW-26 on August 8, 2003, from TW4-20 on August 4, 2005, and from TW4-4 on January 31, 2010. Personnel from Hydro Geo Chern, Inc. were on site to conduct the first phase of the pump test and collect the initial two days of monitoring data for MW-4. EFRI personnel have gathered subsequent water level and pumping data. Analyses of hydraulic parameters and discussions of perched zone hydrogeology near MW-4 has been provided by Hydro Geo Chern in a separate report, dated November 12, 2001, and in the May 26,2004 Final Report on the Long Term Pumping Test. Data collected during the quarter included the following: • Measurement of water levels at MW-4, TW4-19, MW-26, and TW4-20 and, commencing regularly on March 1,2010, TW4-4, on a weekly basis, and at selected temporary wells and permanent monitoring wells on a monthly basis. • Measurement of pumping history, including: pumping rates total pumped volume operational and non-operational periods. • Periodic sampling of pumped water for chloroform and nitrate/nitrite analysis and other constituents 5.3 Water Level Measurements Beginning August 16, 2003, the frequency of water level measurements from MW-4, MW-26, and TW4-19 was reduced to weekly. From commencement of pumping TW4- 20, and regularly after March 1, 2010 for TW 4-4, water levels in these wells have been measured weekly. Depth to groundwater in all other chloroform contaminant investigation wells is monitored monthly. Copies of the weekly Depth to Water monitoring sheets for MW-4, MW-26, TW4-19, TW4-20 and TW4-4 and the monthly Depth to Water monitoring sheets for all of the chloroform contaminant investigation wells are included under Tab C. Monthly depth to water measurements for the quarter are recorded in the Field Data Worksheets included under Tab D. 5.4 Pumping Rates and Volumes Table 2 summarizes the recovered mass of chloroform by well per quarter and historically since the inception of the chloroform recovery program for the five currently- active pumping wells. All of the pumping wells do not pump continuously, but are on a delay device. The wells purge for a set amount of time and then shut off to allow the well to recharge. Water from the pumping wells is transferred to the Cell 1 evaporation pond through a pipeline 19 N:\WMM\Required Reports\Chlorofonn Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroform _ Report_text.doc installed specifically for that purpose. The pumping rates and volumes for each of the pumping wells are shown in Table 3. No operational problems were observed with the well or pumping equipment during the quarter. 5.5 Mass Removed Chloroform removal was estimated as of the first quarter 2007. Since that estimation the mass removed by well for each quarter has been compiled in Table 2, indicating that a total of 614.00 pounds of chloroform have been removed to date. 5.6 Inspections EFRI has submitted an Operations and Maintenance Plan, Chloroform Pumping System, White Mesa Mill, Blanding, Utah, Revision 2.1 which includes a proposed weekly inspection form to UDEQ for approval on October 25,2010. Upon approval of that plan, the Mill will commence documenting its required inspections of the operational status of the chloroform pumping wells on the proposed weekly inspection form. Completed inspections for the quarter, recorded on the approved weekly inspection form, will be included in future Chloroform reports upon approval by UDEQ. At the time of the publication of this report, approval of the Operations and Maintenance Plan, Chloroform Pumping System, White Mesa Mill, Blanding, Utah, Revision 2.1 had not been received. As mentioned above, there were no operational problems in the pumping wells this period. 5.7 Conditions That May Affect Water Levels in Piezometers There no water was added to the any of the wildlife ponds during the quarter. 6.0 CORRECTIVE ACTION REPORT Necessary corrective actions identified during the current monitoring period are described below. Identification and Definition of the Problem TW4-24 receipt pH Appendix A of the QAP states that all VOC samples are required to be preserved and arrive at the laboratory with a pH less than 2. A review of the laboratory data revealed that all VOC samples were received at the laboratory with a pH less than 2 except for one, TW4-24. EFRI was not informed of the issue by the laboratory at the time of analysis. The sample was not recollected, because EFRI became aware of the issue after the end of the second quarter. The laboratory noted the pH was 5 at the time of analysis. It is important to note that the EPA standard holding time for non-preserved VOCs is 7 days. The analysis of TW4-24 was completed by the laboratory within 7 days, which is within the EPA standard hold time for a non-preserved sample. Since the sample was analyzed within EPA required hold time for non-preserved samples, the data are not rejected. 20 N:\ WMM\Required Reports\Chloroform Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroform _Report _text. doc A similar corrective action was identified in the second quarter 2012 sample event. EFRI was able to identify that Field Personnel inadvertently omitted the laboratory-provided preservative, and the issue was addressed with Field Personnel and corrected. Further investigation into the issue showed that the pH of TW 4-24 at the time of sample collection was 6.71. For the laboratory to have received that sample with a pH of 5 would indicate that there was preservative present in the sample bottle. The preservative provided to EFRI Field Personnel is made at and shipped by the laboratory. As this is not the first issue with sample receipt pH, EFRI believes the issue is due to inconsistent preparation of the preservative by the laboratory and is not due to an error by EFRI Field Personnel. Trip Blank Holding Times One of the three trip blanks analyzed during the third quarter of 2012 was outside of the required holding time. All other samples received with the trip blank were analyzed within the required holding time and as such the data are not rejected. The samples arrived at the laboratory with more than sufficient time to analyze all of the samples within the required holding time, and therefore EFRI believes this to be a laboratory error. EFRI was not informed by the laboratory of the holding time issue, and the data package sent to EFRI by the laboratory also did not identify the issue. It was not until EFRI's manual review of holding times that the problem was identified. Assignment of Responsibility for Investigation of the Problem Both problems have been investigated by the QA Manager. Investigation and Determination of Cause of the Problem TW4-24 receipt pH As discussed above, the sample TW4-24 was received by the laboratory with a pH of 5, which is above the QAP required limit of 2. After further investigation, EFRI believes the issue of sample receipt pH is due to inconsistent preparation of the preservative by the laboratory. All other samples were received within acceptable pH levels indicating this is an isolated issue for this one sample. This issue has occurred in the past, and EFRI Field Personnel have been made aware, and actions have been taken to eliminate this problem. As such, EFRI has determined the issue of sample preservation resulted from the source of the preservative, which is the current laboratory. Trip Blank Holding Times As discussed above, the Trip Blank sample collected on 911 0/20 12 was analyzed by the laboratory outside of the required holding time. In a review of the data, EFRI determined the Trip Blank was received by the laboratory on 9114/2012 and not analyzed until 9/26/2012; which resulted in the data being outside the required holding time. 21 N:\ WMM\Required Reports\Chloroform Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroform _Report _text. doc Determination of a Corrective Action to Eliminate the Problem TW4-24 receipt pH The sample which was received at the laboratory with a pH greater than 2 is the result of inconsistent preparation of sample preservative by the laboratory. EFRI has initiated an investigation into contracting an alternative laboratory and expects to make the change for the 1 st quarter 2012 sampling event. Trip Blank Holding Times The Trip Blank sample, which was analyzed outside of required holding time, was a result of a laboratory error. The samples were received with more than sufficient time to analyze all samples within the required holding time. EFRI has determined this issue is due to laboratory error and not due to any actions or inactions by EFRI. As discussed above, EFRI has initiated contract negotiations with an alternate Utah certified analytical laboratory and expects to make the change for the 1 st quarter 2012 sampling event. Assigning and Accepting Responsibility for Implementing the Corrective Action TW 4-24 receipt pH & Trip Blank Holding Times It will be the responsibility of the QA manager to review data from the alternate Utah certified laboratory to assure completion of analysis within the method specified holing times. Implementing the Corrective Action and Evaluating Effectiveness TW 4-24 receipt pH & Trip Blank Holding Times EFRI has contacted the current laboratory to make them aware of the issues. In addition, EFRI has initiated the process to find and change analytical laboratories. The change to a new analytical laboratory is expected to occur prior to the 1 st quarter 2013 sampling event. Once a new laboratory is identified, the sample receipt data will be assessed as samples are received at the new laboratory to determine if any further action is necessary. Verifying That the Corrective Action Has Eliminated the Problem TW 4-24 receipt pH & Trip Blank Holding Times Verification that samples are analyzed within the required holding time, and are received at the laboratory with a pH less than 2, will occur during the assessment of data collected from the first quarter 2013 sampling event. 6.1 Assessment of Previous Quarter's Corrective Actions Chloroform was present in the rinsate blanks and chloride was present in the DIFB during the second quarter 2012. To address previous nitrate contamination in the nitrate and chloroform sampling programs, an additional rinse with 55-gallons of DI water has been added to the decontamination process. The nitrate contamination has been eliminated from rinsate blanks, however, the addition of 55-gallons of DI water has resulted in chloride contamination in rinsates and DIFBs. 22 N: \ WMM\Required Reports\Chloroform Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroform _Report _text. doc The new rinsate requirements under QAP, Revision 7.2, lower the frequency which field personnel collect rinsate samples and allows the DI system to recover. The lower rinsate frequency resulted in no rinsate contamination during the third quarter of 2012. The DIFB for the third quarter of 2012 indicated chloroform was present in the sample, however, EFRI has determined this result is due to laboratory carryover and is not representative of actual contamination in the DI water system. EFRI is making arrangements to contract another laboratory. Rinsate and DIFB data will be reviewed to determine if additional corrections are necessary. f Verification that rinsate and DIFB contamination has been eliminated will occur upon completion of the system upgrades and receipt of at least the two quarters of data. If contamination persists then additional sources will be researched and the investigation will continue. The corrective actions for the second quarter of 2012 also discussed a rinsate sample which was received by the laboratory with a pH greater than acceptable limits. The third quarter of 2012 showed all rinsate samples were received at acceptable limits. However, the sample TW4-24 for the third quarter 2012 sampling event was received by the laboratory with a pH of S. EFRI has investigated this issue and has determined that Field Personnel followed all corrective actions identified during the second quarter of 2012, and the issue is related to inconsistent laboratory preparation of the acid preservative that is provided by the laboratory. These inconsistencies, along with other recurring issues from the current laboratory, have prompted EFRI to find a new laboratory. This change is expected to be implemented for the 1 st quarter 2013 sampling event. 7.0 CONCLUSIONS AND RECOMMENDATIONS The water level contour maps for the third quarter, 2012 indicate effective capture of water containing high chloroform concentrations in the vicinity of pumping wells MW -4, MW-26, TW4-19, and TW4-20. A well-defined capture zone is not evident at TW4-4. The capture zone associated with TW 4-4 is likely obscured by the low water level at adjacent well TW 4-14 and the two orders of magnitude decrease in permeability south of TW 4-4. However, the decrease in chloroform concentrations at TW 4-6 (located downgradient of TW 4-4) since the fourth quarter of 2009 is likely related to TW 4-4 pumpIng. Third quarter, 2012 chloroform concentrations at many of the wells with detected chloroform were within 20% of the values reported during the previous quarter, suggesting that variations are within the range typical for sampling and analytical error. Changes in concentration greater than 20% occurred in wells MW-26, TW4-S, TW4-6, TW4-10, TW4-18, TW4-19, TW4-20, and TW4-22; the concentration in well TW4-27 remained non-detect. Of the wells showing changes in concentration greater than 20%, MW-26, TW4-19, and TW4-20 are pumping wells. TW4-7 is located adjacent to pumping well MW-4; TW4-10 is located adjacent to pumping well MW-26; TW4-S and TW4-22 are located adjacent to pumping well TW4-20; TW4-18 is located adjacent to pumping well TW4-19; and TW4- 6 is located adjacent to pumping well TW4-4. Fluctuations in concentrations at pumping 23 N:\ WJ'vlM\Required Reports\Chloroform Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroform _Report _text. doc wells and wells adjacent to pumping wells likely result in part from changes in pumping. Between the current and previous quarters, the concentration in TW4-26, which is the most downgradient temporary well, increased slightly from 4.1 f.lg/L to 4.9 f.lg/L. The changes in concentrations at TW4-6 and TW4-26 are likely the result of their location near the downgradient edge of the plume where changes in upgradient pumping are expected to affect concentrations. The highest chloroform concentration (13,000 f.lg/L) was detected at pumping well TW4- 20. Since the last quarter, the chloroform concentration in TW4-20 decreased from 36,000 f.lg/L to 13,000 f.lg/L, the concentration in adjacent pumping well TW4-19 increased from 460 f.lg/L to 950 f.lg/L, the concentration in nearby well TW4-21 increased slightly from 400 to 410 f.lg/L, and the concentration in nearby well TW4-22 increased from 120 f.lg/L to 940 Jlg/L Fluctuations in concentrations in these wells are likely related to their location near the suspected former office leach field source area in addition to variations in pumping in TW4-20 and nearby wells. Regardless of these measured fluctuations in chloroform concentrations, sampling of temporary wells TW 4-24 (located west of TW4-22) and TW4-25 (located north of TW4-21), indicates these wells remain outside the chloroform plume and thus bound the plume to the west and north. Chloroform was not detected at TW 4-25 and was detected at a concentration of 1.1 f.lg/L at TW4-24. The chloroform concentration at well TW4-6 increased from 4.7 f.lg/L to 6.9 f.lg/L. This well has been outside the chloroform plume boundary since the fourth quarter of2010. In the past, TW 4-6 has been both within and outside the plume. From the first quarter of 2009 through the fourth quarter of 2010, TW 4-6 was within the plume. Prior to that time, between the time of installation in the second quarter of 2000 and the fourth quarter of 2008, TW 4-6 was outside the plume. Although fluctuations in concentrations have occurred, this well likely remained outside the plume between installation in 2000 and the fourth quarter of 2008 due to a combination of 1) slow rates of downgradient chloroform migration in this area due to low permeability conditions and the effects of upgradient chloroform removal by pumping, and 2) natural attenuation. The decreases in concentrations at TW 4-6 since the fourth quarter of 2009 are likely the result of upgradient pumping, in particular pumping at adjacent well TW4-4 (which commenced in the first quarter of 2010). Chloroform remained non-detect at downgradient temporary well TW4-23. TW4-23 and TW4-6 (with a chloroform concentration of 6.9 f.lg/L) bound the chloroform plume to the south. TW4-8, TW4-12, TW4-13, TW4-14, and TW4-27 bound the chloroform plume to the east. Continued pumping of MW-4, MW-26, TW4-19, and TW4-20 is recommended. Pumping these wells, regardless of any short term fluctuations in concentrations detected at the wells (such as at TW4-20), helps to reduce downgradient chloroform migration by removing chloroform mass and reducing average hydraulic gradients, thereby allowing natural attenuation to be more effective. Continued pumping at TW 4-4 is also recommended to improve capture of chloroform to the extent practical in the southern portion of the plume where low permeability conditions exist. The general decrease in chloroform concentrations at TW4-6 from 1000 f.lg/L to 6.9 f.lg/L since the first quarter of 2010 is likely related to pumping at TW4-4. The decrease in the long-term rate of water level rise at TW 4-6 since TW 4-4 pumping began, which suggests that TW 4-6 is within 24 N:\ WMM\Required Reports\Chloroform Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroform _Report _text. doc the hydraulic influence of TW 4-4, IS consistent with the decrease In chloroform concentrations at TW 4-6. 8.0 ELECTRONIC DATA FILES AND FORMAT EFRI has provided to the Executive Secretary an electronic copy of all laboratory results for groundwater quality monitoring conducted under the chloroform contaminant investigation during the quarter, in Comma Separated Values (CSV) format. A copy of the transmittal e-mail is included under Tab M. 25 N:\ WMM\Required Reports\Chloroform Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroform _Report _text.doc 9.0 SIGNATURE AND CERTIFICATION This document was prepared by Energy Fuels Resources (USA) Inc. on November 27, 2012 Energy Fuels Resources (USA) Inc. By: David . Fry enlund Senior Vice President, Regulatory Affairs and General Counsel 26 N:\WMM\Required Reports\Chlorofonn Quarterly Monitoring Report\2012 Q3\2012_ Q3Chloroform_Report_text.doc Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penal . es for submitting false information, including the possibility of fine and impriso~nt fj knowing violations. Davi . Fry enlund Senior Vice President, Regulatory Affairs and General Counsel Energy Fuels Resources (USA) Inc. 27 N:\ WMM\Required Reports\Chloroform Quarterly Monitoring Report\20 12 Q3\20 12_ Q3Chioroforrn _Report _text. doc Tables Table I: Summary of Well Sampling for the Period ",,;;,",, 1"'''' ',~""I(l?" ' ':!;iT • I,i%~ (5 1:,,5i'~;:7 ',~r ~,~": ,: -.f'~,L"_~~"; ,I -'~,"~ _ _:~j7 7~,'.,'fj,; , ,,-'r.t ",~ ,:;~ Well,,,;;' ,,,,;, ';;~i%' " !1j '" .. -Sanl',:le Date: '~'Nlf~ lli '.Date"oft:~b ~el1or~,\ih MW-04 9/4/2012 9/25/2012 TW4-01 9/13/2012 1011/2012 TW4-02 9/13/2012 1011/2012 TW4-03 8/29/2012 911212012 TW4-03R 8/28/2012 911212012 TW4-04 9/4/2012 9/25/2012 TW4-05 9111/2012 1011/2012 TW4-06 9111/2012 1011/2012 TW4-07 9/13/2012 1011/2012 TW4-08 8/29/2012 911212012 TW4-09 8/30/2012 9112/2012 TW4-10 9112/2012 1011/2012 TW4-11 9113/2012 1011/2012 TW4-12 8/2912012 911212012 TW4-13 8/29/2012 9/12/2012 TW4-14 8/29/2012 911212012 MW-26 9/4/2012 9/25/2012 TW4-16 8/30/2012 9112/2012 MW-32 9/5/2012 9/25/2012 TW4-18 9111/2012 1011/2012 TW4-19 9/5/2012 9/25/2012 TW4-20 9/4/2012 9/25/2012 TW4-21 9/13/2012 1011/2012 TW4-22 9/12/2012 101112012 TW4-23 8/29/2012 9/12/2012 TW4-24 8/30/2012 9/12/2012 TW4-25 9111/2012 10/1/2012 TW4-25R 911012012 10/1/2012 TW4-26 9111/2012 10/1/2012 TW4-27 8/30/2012 9112/2012 TW4-60 9113/2012 1011/2012 TW4-65 9/5/2012 9/25/2012 TW4-70 9/11/2012 10/1/2012 All sample locations were sampled for ChlorofonTI, Carbon Tetrachloride, Chloromethane, Methylene Chloride, Chloride and Nitrogen "R" following a well number deisgnates a rinsate sample collected prior to purging of the well of that number. TW4-60 is a DI Field Blank, MW-65 is a duplicate of MW-32, and TW4-70 is a duplicate of TW4-25 , Highlighted wells are continuously pumped, Table 2 Chloroform Mass Removal Per Well Per Quarter T~4-15 (MW-26) . TW4-19 TW4-20 · TW4-4 ' . Quarter MW-4 (Ibs.) (Ibs.) (Ibs.) . (Ibs.) (Ibs.) ,Quarter Totals (Ibs.) Q12007 36.8 12.9 150.2 87.0 NA 286.9 Q22007 1.4 0.1 0.0 2.5 NA 4.0 Q32007 2.2 0.8 2.9 3.1 NA 9.0 Q42007 1.7 1.0 3.1 4.8 NA 10.6 Q12008 1.7 0.4 4.6 7.2 NA 13.8 Q22008 1.3 0.5 3.2 9.9 NA 14.8 Q32008 1.2 0.3 15.9 9.3 NA 26.8 Q42008 1.3 0.3 20.7 0.4 NA 22.7 Q12009 1.7 0.4 4.3 3.6 NA 10.0 Q22009 6.8 0.2 3.7 2.8 NA 13.5 Q32009 1.5 0.4 11.1 5.5 NA 18.5 Q42009 4.8 0.6 17.8 26.1 NA 49.4 Q12010 0.9 0.4 2.7 0.4 NA 4.5 Q22010 1.5 1.0 6.8 5.9 1.4 16.5 Q32010 1.3 1.2 2.0 4.9 1.3 10.6 Q42010 1.1 0.5 7.7 7.4 1.2 17.9 Q12011 1.1 0.2 12.9 9.6 1.1 24.9 Q22011 1.2 0.8 5.3 4.6 1.1 13.1 Q32011 1.2 0.4 1.1 4.1 1.2 8.1 Q42011 1.2 0.8 2.7 4.8 1.4 10.9 Q12012 1.1 0.6 0.8 7.0 1.0 10.5 Q22012 1.1 0.6 0.7 6.9 1.1 10.4 Q32012 1.1 0.7 1.4 2.4 1.1 6.7 Well Totals (pounds) 75.1 25.1 281.5 220.2 12.0 614.0 Table 3 Chloroform Well Pumping Rates and Volumes Volume of Water Pumped Pumping Well Name during the quarter (gals) Average Pump Rate (gpm) MW-4 91,607 4.3 MW-26 25,246 10.9 "--TW4-4 80,006 9.1 TW4-19 171,345 14 TW4-20 22,025 lOA Tab A Site Plan and Perched Well Locations White Mesa Site MW-5 • perched monitoring well TW4-12 o temporary perched monitoring well TWN-10 <> temporary perched nitrate monitoring well PIEZ-1 ~ TW4-27 ~ perched piezometer temporary perched monitoring well installed October, 2011 RUIN SPRING o seep or spring HYDRO GEO CHEM, INC. WHITE MESA SITE PLAN SHOWING LOCATIONS OF PERCHED WELLS AND PIEZOMETERS DATE REFERENCE H:/718000/may121Uwelloc12.srf .-V FIGURE A-1 TabB Order of Sampling and Field Data Worksheets \"" .' Order of Contamination for 3rd Quarter 2012 Chloroform Purging Event Chloroform Well Sample time Levels Rinsate date/time TW4-03 ff/:J-q I J:l. t)l26 ND TW4-12 () bY$" ND TW4-13 6 6 ~'",-Z;' ND TW4-14 6706 ND MW-32 9/5 13l-{o ND TW4-23 0913 ND TW4-08 0'12.5: ND TW4-09 ~/Jpii 2 061-/0 ND TW4-16 D6£;Q ND TW4-24 D700 ND TW4-27 07i2 ND .::is R TW4-25 q/l)/12 06!>O ND 1/IO/1...DI1. }C):2.0 TW4-26 D70g 4.1 TW4-06 07:li 4.7 TW4-05 073S 8.4 TW4-18 D7Y7 24 TW4-10 41u112 O~1C7 79 TW4-22 o."21'-o·7~?. 120 TW 4-21 "/t'lI12.. 0, 'is 400 TW4-19 9151/'2 10:10 460 TW4-11 1/1'1 0(;57 660 TW 4-07 G\! \3 0'70," 790 TW 4-01 4/1'~ 0 7 11 1000 MW -04 q I y I j 1 \ Y iD 1400 TW4-04 q/y/; '2. lli ;~(' 1500 TW4-02 Q/1'3/12. 0"'36 2500 MW-26 t) /11/1 a. 13Gb 3000 TW4-20 q It-til J 13:>5 36000 TW4-60 0.1. Blank 0\/)3/12 08.s..5 TW4-65 Duplicate t1 t,j-3.1 4/s, i 3t.i D TW4-70 Duplicate ~\2S-~ Comments: lWt.1-~S Name: Water Well level Depth Date: 141 101.5 102.5 93 130.6 Bladder pump 114 125 120 142 112.5 96 134.8 86 97.5 120 137.5 111 113.5 121 125 Cont. Pumping 100 120 110 124 Cont. Pumping 112 Cont. Pumping 120 122.5 Cont. Pumping 106 Cont. Pumping Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL !:~;;;~;I)~-~I FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 ?/tA: QUllrh:r C.h loro-t6rM 201?.. ~ See instruction Location (well name): L-I _M_W_-_O_'-I...:..-_________ --I Sampler Name and initials: 1 r::r;.nn<r gol1;J~/-rl+ Field Sample ID Date and Time for Purging ..... 1 ......;~_I_~_1_2_o_1_?-, ____ ---' and Sampling (if different) 'V/A '------------~ Well Purging Equip Used: ~pump or [QJ bailer Well Pump (if other than Bennet) 1 Go..,.:}muo\A..,) Purging Method Used: [QJ2 casings [QJ3 casings Sampling Event 1 Q"",o.rfe(' lj Ch Jor~ "'W\ Prevo Well Sampled in Sampling Event ..... 1_}J._w_-.2._£ ______ ~ pH Buffer 7.0 7.0 Specific Conductance L-I _l\,:..tt_1 ___ ---'1 ~MHOS/ cm Depth to Water Before Purging 17 S. g S Conductance (avg) 1~ '1 L--__ ~~ _____ ~ pH Buffer 4.0 '1.0 Well Depth(O.Olft): 1.-1 _0 _' • ___ ----' 12'-\.DO Casing Volume (V) pH of Water (avg) 4" well:1 3" Well: /.J8 () 1(·653h) '17. b 7 ,c.367h) Well Water Temp. (avg) 1 1 '.1 g Redox Potential (Eh) 10-1 _j ~_3 __ ~ TurbidityL-I_() ___ ...... Weather Condo ..... 1 __ S_"'_V\_h_~""""__ ________ ____' Ext'l Amb. Temp. O( (prior sampling event) 10-1 _2...;;;.,g_f)_----I Time 1 1 '1 0'\ Gal. Purged Time Gal. Purged Conductance ..... 1 _F-_\'_1 __ ...... pH 11.\K Conductance pH ...... 1 __ ----' Temp.oC Temp.oC Redox Potential Eh (mV) lb3 Redox Potential Eh (m V) ..... 1 ____ ...... Turbidity (NTU) o Turbidity (NTU) Time Gal. Purged Time Gal. Purged Conductance pH Conductance pH 11.--__ ----1 Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (m V) 11.--___ .....1 Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60= I Y.3 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T=2V/Q= I 0 I I t> N arne of Certified Analytical Laboratory if Other Than Energy Labs ..... 1 ~--..:...1...;..A~ _____ ----, Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y VOCs III D 3x40 ml D ~ HCL [g) Nutrients ~ D 100 ml D It! H2SO4 ~ Heavy Metals D D 250 ml D D HN03 D All Other Non Radiologics D D 250 ml D D No Preserv. D Gross Alpha D D 1,000 ml D D HN03 D Other (specify) It! D Sample volume D IJ D Gh\or~~L If preservative is used, specify Type and Quantity of Preservative: Final Depth ..... 1 _7 _7_, 1_q_. __ --' Sample Time 1.-1...:..' 4....:.;1:...:::;0 __ -, See instruction Comment A;r .. ;-.JeA On SI~G ~t-lYOQ. ~f\n.c/ ~fla ~rri,., pr~sC'l'\.y +0 coJ)e.d-.5Q.(II)FJt:~. ~ ~""p\(..S ~o\l.ec+t:J 6-T ILJlO, w ~tc:"" ~"'~ CJ~r. L crt s ; t r. (A 1-1 ~ )y MW-0409-04-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D ~ 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) OENISONI),4,4 MINES Description of Sampling Event: ATTACHlVIENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 1 3'('"&>: GI"'IA.;:t~(" C'h 1 o.04~, yv\ 20 \2. ~ See instruction Location (well name): Io.-1-r_w_4_-_0_1 _________ ---' Sampler Name and initials: 1 =r~t'\(Ier fJolJ:J~/fH Field Sample ill Date and Time for Purging ...... lqt.L.l...:...l~_I_2._()..;..l~..;;;:,..... ____ --' and Sampling (if different) 4/13/~012.. Well Purging Equip Used: Iltl Ipump or [QJ bailer Well Pump (if other than Bennet) 16runa:to.s Purging Method Used: [![]2 casings [QJ3 casings Sampling Event IQv.Q.("fGf'"k1 Chlo;:r)fo(W) Prevo Well Sampled in Sampling Event I ..... _,,_W_Y_ .... _D_7 _____ ....I pH Buffer 7.0 ..... 1 _7_._0 ___ .....1 Specific Conductance 1-1 _'1...:,..q:....q'--__ ---'I /-tMHOS/ cm Depth to Water Before Purging 1 ''1 170 Conductance (avg) .2 J 52-"'-----------------------' pH Buffer 4.0 Well Depth(O.Olft): 1 11 D, OD Casing Volume (V) pH of Water (avg) 4" well:1 ~q .58 IC.653h) 3" Well: ...... .....;o~ __ ....1_(.367h) Well Water Temp. (avg) 1 19 I bE) Weather Condo I c.I ou~tJ v.J i-tl.c 'R""~,, Redox Potential (Eh)1 ;L '-\& Turbidityl ..... 1 __ 3......;~ __ ...... Time 1 1395 Gal. Purged Conductance I ~ 1 1..\6 Temp.oC Redox Potential Eh (m V) ...... 1 ,2~Q'-ll:...-_.....I Turbidity (NTU) 1 12>J Time 1 l'311S Gal. Purged 1 ..... 5_D ___ ...... Conductance 1 21 S } pH I t;.Zj Temp. °C I ] LJ. &;1 Redox Potential Eh (m V) ..... 1 _~_t:::)_7_-.....I Turbidity (NTU) 1 140 White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event}1 C22 () Time 1 ~'3'14 Conductance 1 2..J55 Temp.oC Gal. Purged ..... 1 _y_o __ ...... pH 1 bIT! Redox Potential Eh (m V) ..... 125 __ 0 __ ...... Turbidity (NTU) Time I r3QZ: Conductance I ~JS3 Temp.oC 1 )~ ,eg 11'3>'1 I Gal. Purged ..... 1 _'_0 __ .....1 pH 1 '.~Cj Redox Potential Eh (mV) ..... 12_45 ___ .....1 Turbidity (NTU) 1193 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged ('0 gallon{s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1-1 ..:...:\O~ __ ----J Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V/Q = 1 5, l\' I o o Name of Certified Analytical Laboratory if Other Than Energy Labs L.:.IN....;...!,./...:...A.:...-_____ ----I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y VOCs 1il 0 3x40 ml 0 "'fl HCL ~ Nutrients ~ 0 100 ml 0 ~ H2SO4 ~ Heavy Metals 0 0 250 ml 0 0 HN03 0 All Other Non Radiologies 0 0 250 ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) "'f] 0 Sample volume 0 lJ 0 Ch'or~A~ If preservative is used, specify Type and Quantity of Preservative: Final Depth 11Db. S3 Sample Time 0717 Comment ~ See instruction A r r: \j.A 01\ ~;.j. "-... + 13:3>". -J,." lI ... r "n J. 6-"r,; n p ""5Cf1 t--tor flAr~ ~. Pw" ~ <-h e~ <VI. o.t J :3 YO, f \J. (~<! 4 IN e H -ft.( (, M i/ll,q.G S. \.0 "'-\-or """'-So a ; ,..-t~ wITh S.;.oIe 5,,~ 4 F"+' <Jc.s . N 0 0 0 0 0 tJ P~r~t:.-eYlae~ ~-t 13Yfo. Lt:-f} ~Ii-C ttl-135J.. Arr:-.1-c.d.. Ol'\ ~;t~ ~+ 07tD .1A..P'\n-<T o.nJ. tra . .t"r-,'f\ pr~ent ~6 Golled' 5Cc.MfJ~s... D~f>-th +0 b-.)C4..,.fer Wa.$ GY.'1D" S"-rY\p)o bt>..:'e.~ ""+ o=rer7 07J7. L-e,-f1-5.\:tv J' D7~) TW4-0109-12-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ~ See instruction Location (well name): .... 11--.:;.\N...;...L....L\-_D_2. _________ ----I Sampler Name and initials: l:::=tt)ner HDI ha~J(H Field Sample ID Date and Time for Purging I ~J\2.7~01'2.." and Sampling (if different) ~JI37a.ol~ Well Purging Equip Used: ~pump or [gJ bailer Well Pump (if other than Bennet) I Crf\A() ar-OS Purging Method Used: ~2 casings [gJ3 casings Sampling Event IQ ",-().rfer~ 6~lofbfo,Y\'\ Prevo Well Sampled in Sampling Event I .... l'W __ t1..,.....--'_O_' ____ ----I pH Buffer 7.0 7.0 pH Buffer 4.0 Specific Conductance .... 1 _4...:..q_11--__ ----I1 ~MHOS/ cm Well Depth(O.Olft): 1 12.D. 00 Depth to Water Before Purging I b I, 30 Casing Volume (V) 4" well:1 ~~.~\ 1(·653h) 3" Well: () (.367h) 1...-""--__ --' Conductance (avg) :>S 3 ~ pH of Water (avg) b .70 1...-____________ ----1 Well Water Temp. (avg) I \ q ,1 ~ Weather Condo I [.\ov..~ wrl-h '''''f) Redox Potential (Eh)1 'J-IO TurbiditylL-...:...\tl_S __ --' Time I \'l~O Gal. Purged I S 7. 'E>D Conductance I '3.532.. pH (;.70 Temp.oC IP-l.7Q Redox Potential Eh (mV) 1L-::x"--:7_D __ ...... Turbidity (NTU) 1 1 liS Time 107'3"0 Gal. Purged Conductance pH IG.&9 Temp.oC Redox Potential Eh (mV) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event)I 2...?..o Time Gal. Purged Conductance pH I '--__ -----' Temp.oC Redox Potential Eh (mV) 1 .... ___ --' Turbidity (NTU) Time 1 O"~Q. Conductance 1 A 4 4 ~ Temp.oC Gal. Purged .... 1 _0 __ ---' pH 1 G.gl Redox Potential Eh (m V) .... 1 :2.._'"0 __ --' Turbidity (NTU) 1 8.3 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Be1-~,e V olume of Water Purged Sf,SD gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I 10 T=2V/Q= I b,gS I Number of casing volumes evacuated (if other than two) 11,£7 If well evacuated to dryness, number of gallons evacuated 157.56 I N arne of Certified Analytical Laboratory if Other Than Energy Labs ,tV I A ~--------------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs ~ D 3x40 ml D ~ HCL t;a D Nutrients ~ D 100 ml D [J H2SO4 00 D Heavy Metals D D 250ml D D HN03 D D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) ~ D Sample volume D ~ D rg C h\b('~~ If preservative is used, specify Type and Quantity of Preservative: Final Depth 1 .......... \ \--,~,-,-\_OD~ __ --, Sample Time Comment ~ See instruction A rri ve4 on ~ 11-<:.. ",1-\ '130. "'" r>~'-OJ) J.. &t>J'ri" f'i'GS.~ -tor f' lA(,~ e . 'P v..~ e ~ M "'-+- 1'-1 ::?:,]:, . 'P v-r ~ e,l wen -to r 0.... + C>+6..1 0+ .5 I'Vl ;" u\;Tu "1.1'1 J. ys 5~c.OI)Js, f IA~C J v.) el ) ~ f~. 1..:>0..1-Gr ~(i..S. tyl \,\.,-~ • l-e.+Y.s I rc-J-~ . P \A.r~ c. en j e.J "L + I ~ '-l D A~r>'v-c.d.. Clt'\ S ;+" ~+ 072], lAM.r "",.I. G-o..rr;/\ prese~t'-iS fo Gollec.1-S'V'1[,it:.s., Pep+4 +0 v.:>cJ--tf' V-)~~ b 7 .£:2.. S~p1~ bd\\\~a ~t 0730. ~ e-R-~l~h:, P\.-r 01 '33 TW4-0209-12-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 . ~ See instruction OENISON~~~ WHITE MESA URANIUM MILL MINF;S FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 -srdl Qv.o,rfe.r Ghlor-O+orn'\ a.D12.. Location (well name): 1-1-rw __ 11_--_D_3 __________ ---' Sampler Name and initials: 1 ~)'l(\er Ho]),J",~;rn Field Sample ill Date and Time for Purging 1 ~ } 2.. g 7,2() 1 '<. and Sampling (if different) '-1_g_7a.._4_J.:2._0_'~ _____ ----' Well Purging Equip Used: ~pump or @] bailer Well Pump (if other than Bennet) 1 &rlAn(ffo5 Purging Method Used: [][]2 casings @]3 casings Sampling Event IG""o..<+U"I~ c..hlo-rO*of'rY\ l-nJ.> Y-03 1<. Prevo Well Sampled in Sampling Event '--_________ ...... pH Buffer 7.0 1-1 _,_,_0 ___ ----1 pH Buffer 4.0 q.o Specific Conductance 1-1 _4_1_~ ____ .....I1 ~MHOS/ cm Well Depth(O.O 1 ft):1 L.-_1 q_l_. 0_0 __ ----1 Depth to Water Before Purging 1 SO. , g 4" well:1 5~ :~O 1(.653h) 3" Well: 0 (.367h) '---------I Casing Volume (V) Conductance (avg) ;2.. '-\ ')...0 '---~-------~ pH of Water (avg) L..-..:~""-._S_/~ _____ --' Well Water Temp. (avg) '\1, Ol Redox Potential (Eh), :;2... "15 Turbidity'-:3 O. 5 Weather cond'l L.-_~_o..._r~_'_~ __ G_\ o_v._~_~ ____ ----, Time ,0816 Gal. Purged L.-I 4_0 ___ --' Conductance pH C:>.S 1 Temp.oC \7.6 1 Redox Potential Eh (m V) 1,---~_~_5 __ --I Turbidity (NTU) Time I OGXC Gal. Purged Conductance JS8q pH Temp.oC }£" 11 q Redox Potential Eh (mV) Turbidity (NTU) D White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event)IL.-;:2._0_o __ ...... Time Gal. Purged Conductance pH I'--__ ~ Temp.oC Redox Potential Eh (m V)I '--___ ---' Turbidity (NTU) Time I C1:~:"·~(.i I 007 Conductance Temp.oC Gal. Purged 1£71 J5 .. '17 1 Redox Potential Eh (mV) 1 .3 t1 g Turbidity (NTU) 6 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) [? "{!.If Ole, Volume of Water Purged 1~'toMD~-------' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I \0 T = 2V /Q = I I \. g(' I Number of casing volumes evacuated (if other than two) 1),51 If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs L-I ""_I A _______ --' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs ~ 0 3x40 ml 0 ~ HCL ~ 0 Nutrients l:l 0 100 ml 0 rtI H2SO4 l:l 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) 1l;I 0 Sample volume 0 ~ 0 ~ Gh \D('i~e. If preservative is used, specify Type and Quantity of Preservative: Final Depth I \ L.} 0 . 0 t> Sample Time Comment ~ See instruction A("'r;\Je~ 0'(\ ~I't~ 0.+ 080.a.... T"'f'I)'\l:!("" "f\~ c;.~r(';(\ fl"-E!.~en+ -tor" f\.A('~e. ?V\r~e be~CIV1 0\.+ Og(J7 P \A,f"~e~ \N en .for-"'m~1\v\.1e~. '?v..r~'G~ v.::>(.1l j,(~ : \NA.1-~(' ~ o.,s '(Y1 o.s+8 CJ-e.tI\(', ?"'r~ c.r'\de~ fA' 0 g \~. ~e..r1--sit~ tAt og;2.1 /lrr\ve~ 0(\ .sIt!. 0-..1-Ob)...O. -r;.t'\t'\'iU ~"J.. CrOl..rn'T\ f'('e..s.~".t-..j.o c¢}}ec1-~~fVl1J-e.s.· P"<P~ +t> w~1-er 'lilA> SO. I g. So.rY\ P )0 b..llca. ",1-0 b~ • Lm .$'+<:" "t-0630 TW4-0308-28-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL [--------_. __ ._-_ ... _. __ .... _, i OENISONI)~~1 L MINES . I FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 3 rJ Qu.o..rfer Ghlorofbf'/V) :;2.01~ ~ See instruction Location (well name): 1'---'T_W_4_-0_3....;R~ ________ ---I Sampler Name and initials: I -'-;'nner YoJ1;J~./TB- Field Sample ill Date and Time for Purging I S/9..8'/2.01~ and Sampling (if different) L...;I M~Y...;.;~~ _______ --J Well Purging Equip Used: I]I]pump or [9] bailer Well Pump (if other than Bennet) 16-r\AnMs Purging Method Used: [9]2 casings [9]3 casings Sampling Event I Q"",.h,-lct eh I".... Ot:;,fM Prev. Well Sampled in Sampling Event 1 ..... ·_N_Yi_ft ________ ...... pH Buffer 7.0 7.0 Specific Conductance I ..... _'f_'l....;..~ ___ ---II ~MHOS/ cm Depth to Water Before Purging r...-I _0 ___ .... Conductance (avg) ~.1 ~-=-~--------I pH Buffer 4.0 Y.D Well Depth(O.Olft): o Casing Volume (V) pH of Water (avg) 4" well:~_o __ --II(.653h) 3" Well:. () . (.367h) 6.SY Well Water Temp. (avg) 1 .2:1< bb Redox Potential (Eh)1 2~ Turbidity ,-I ....;.;.G..;...;.5~_ ...... Weather Condo Ext'l Amb. Temp. O( (prior sampling event)I ..... ~_o_b __ ...... Time ,-10;....:7:......3"'-1.1 __ ...... Gal. Purged ,-I ...:...)~.;..;;;O __ ---.J Time Gal. Purged Conductance l ..... b..;........:.l'---_---' pH I b.:;lj Conductance pH IL--__ ....... Temp.oC Temp.oC Redox Potential Eh (mV) 1'---.2;..;:;3....::;';),.--'=--_---' Redox Potential Eh (m V) 11-.-___ ...... Turbidity (NTU) 10.5 Turbidity (NTU) Time Gal. Purged Time Gal. Purged Conductance pH Conductance pH 1 ..... ___ .... Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (m V) ..... 1 ___ ---' Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) V olume of Water Purged 150 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = ...... 1 --!., ~O ___ ---, T=2V/Q= 1 0 I Number of casing volumes evacuated (if other than two) 1 0 If well evacuated to dryness, number of gallons evacuated 1 ~ N arne of Certified Analytical Laboratory if Other Than Energy Labs /'1/11 ~~~----------........." Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs ~ 0 3x40 ml 0 ~ HCL ~ Nutrients ~ 0 100 ml 0 ~ H2SO4 ~ Heavy Metals 0 0 250 ml 0 0 HN03 0 All Other Non Radiologics 0 0 250 ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) ~ 0 Sample volume 0 ~ 0 C h 1ov--ide If preservative is used, specify Type and Quantity of Preservative: Final Depth .... 1 __ 0 ________ ----' Sample Time 1,--'; HC_':::' ~..;;;..)_., _. ____ ----' Comment ~ See instruction hr,..hle.~ 01\ Sl'te "".j-07 \~. '"l;..nrver--I\n~ (,-o..("("·n 'f>'f"'e.s:eYJ"f ~r 1>JY1.sClt~- 1<.~n~t1..1-~ b~~OI.Y\ ~1 0/1-6. fu.r'\f>~~ SO &",)loYl~ of .sOGtf lo~h:J titt1J. Joo of DT: ~CA.+c" ~\V\~OL+~ eY)J,e~ ~tla .sG\VV)fl~ c.o}]ecr-eA ~t 07~. Le-F+ S)1-(' ~+ 07'15. TW4-03R 08-28-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2 of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) , .................................... _ .... _._ ..• _._-------, i I>ENISONII)~~1 . ~ MINI:S ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I 3 r (}l Q""o.'+~r ChlCJI'"CJ::ror-tlf' :z.o12 Sampler Name ~ See instruction Location (well name): .... 1 ~..:-..:.W.;;;..~--'---..;:;.O_4.:...... ________ ____' and initials: I ~l1n~r y,,) )1~~~/rH Field Sample ID Date and Time for Purging .... 1 _'1;.:..7_Y~/_2_0..;...1'2. _____ --, and Sampling (if different) Well Purging Equip Used: []!]pump or [gJ bailer Well Pump (if other than Bennet) 11......:-!f1_,',_J _(_.> ..... ' 'i-:..l ____ .--I Gov)'ti t'}\.1 OlA-S Purging Method Used: [gJ2 casings [gJ3 casings Sampling Event I Q\M..r+-e(")~ C~lOf"~r)1l] Prevo Well Sampled in Sampling Event L...I_M_W_-_O_lf ______ ...... pH Buffer 7.0 /.0 pH Buffer 4.0 Specific Conductance L...I _t1J;...;..1..:..~ ___ ---II ~MHOS/ cm Well Depth(O.O 1 ft): ..... 1 1_):2._, 0_0 __ ____' Depth to Water Before Purging I c4tr:trr ' (;4.9D 4" well:I l-bi'':15~ 1(·653h) 2..7,44 3" Well: () (.367h) L...-___ --I Casing Volume (V) Conductance (avg) :l.~ SO L--_~ ______ --' pH of Water (avg) Well Water Temp. (avg) &-1 ~l (,_._l~ __ --I Redox Potential (Eh)1 1q~ TurbiditYL...1 _O ___ ...J Weather Condo L...I_S_V>-_""_r'\_) _________ -.--I Ext'l Amb. Temp. O( (prior sampling event) 1&-2.....;..;;;.9_°_---1 Time Gal. Purged D Time Gal. Purged Conductance I ;2..5:50 Conductance pH L-I __ ----I Temp.oC Temp.oC Redox Potential Eh (m V) L...1 _1~_':L ___ .....1 Redox Potential Eh (m V) IL...-___ ...... Turbidity (NTU) o Turbidity (NTU) Time Gal. Purged Time Gal. Purged Conductance pH Conductance pH 1"'--__ ---' Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (m V) ..... 1 ___ ---' Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = IL..-.-;;~:-.--,L-l __ ----I T=2V/Q= I t) I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs 1a....;.".J,---.;;.~_/t ______ ----' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs Il D 3x40 ml D D1I HCL ~ D Nutrients ~ D 100 ml D ~ H2SO4 ~ D Heavy Metals D D 250ml D D HN03 D D All Other Non Radiologics D D 250m! 0 D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) ~ D Sample volume D ~ D ~ C h \ or~je.. If preservative is used, specify Type and Quantity of Preservative: Final Depth ..... 1 ..... 7_'i_, '1_3 ___ --' Sample Time ..... 1 ..... )~..:..;2.5 ___ ---' See instruction Comment TW4-0409-04-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ~ See instruction Location (well name): L-I _T..:..-v.)_Ll_-_O_5 _________ .....I Sampler Name and initials: I ""~,..ner' »oIJ;J-\j Jilt Field Sample ID Date and Time for Purging I ~!l()1.1.612.. Well Purging Equip Used: (]!]pump or [QJ bailer Purging Method Used: ~2 casings [QJ3 casings pH Buffer 7.0 7.D Specific Conductance L-l _q_tf_~ ___ ---II ~MHOS/ cm Depth to Water Before Purging I 5b . b g Conductance (avg) a........llL.-'1_9..:...1)~ _____ ---' and Sampling (if different) I ~JJI /a.Dl~ Well Pump (if other than Bennet) I-rWt4-' tJ' Prevo Well Sampled in Sampling Event L-_________ .....I pH Buffer 4.0 I q.D Well Depth(O.Olft): I J2.D.Ob Casing Volume (V) pH of Water (avg) 4" well:1 14 1.3L l 1(·653h) 3" Well: 0 (.367h) L--___ ..... Well Water Temp. (avg) I ts :15 Redox Potential (Eh)Ia=~-=-.;;;..g_----, TurbiditylL-)_.35 __ ----, WeatherCond. I l' ~ CID",Jt Ext'l Amb. Temp. O( (prior sampling event)L-12 ___ g.;...o __ -, Time 11QXg Gal. Purged Time PQ2tt Gal. Purged ..... 1 _7_o __ ..... Conductance pH Conductance Temp.oC Temp.oC 1.5.1.5 Redox Potential Eh (mV) Redox Potential Eh (m V) ..... 1 2.9_A..:...-_----' Turbidity (NTU) 1'30 Turbidity (NTU) Time I J'130 Gal. Purged L--Zu.;O:...-_----' Time 1 1931 Gal. Purged ..... 1 -,-1 .;:;...1) __ ..... Conductance ) 484 pH L-I b_,..;."~_----, Conductance 1 19 &7 pH ..... 1 b_._6Z1 __ ..... Temp.oC 15."13 Temp.oC Redox Potential Eh (m V) tLS7 Redox Potential Eh (m V) ..... 1 ~--.;;..;_2 __ ..... Turbidity (NTU) 1'3> 7 Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1--1 _1_0 ___ --1 T = 2V/Q = 1 g . .2..' I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs IV/4 ~--------------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs 1:1 D 3x40 ml D E HCL 'g] D Nutrients 1f1 D 100 ml D lJ H2SO4 ~ D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) lID D Sample volume D ~ D ~ 0hlo('~ d(' If preservative is used, specify Type and Quantity of Preservative: Final Depth 1 514~ Sample Time 073S Comment ~ See instruction Arr, .. j"ed 0"(\ ~a~ a:1-P"H g -r~~t'\Q"" "'(}~ &~tr\~ f .... ~e~ -hr p\>..re:r-. 'Pv.r-~-c.. b~O\r'\ 4 J 1..}2.~ 'P\AC'"~e~ ~cn +0 f' fA. -tr,1-o...\ S q Yl'J1'fJ\A.1<.5. wo..1--tr t,.j~ Mu"( k.~ ?v..r~<. e,tJea od-1L\'3J l~ $l't-< iA1 l~ 3'1. Ar('l'\)~ 01'\ Sl~t:. ~t D"1:1...7. ~t'\"U" o.f\~ G-~rriV) p('es.~ to Goll~d .. s~M'pI~~. ()(!P~ ~ we...h~r WAS 5t:,.bi:f SI\~f>'e6 6~;\~c\ J-07~5 \ Len .$.(tG "'-t 07~4 TW4-0509-10-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) j)ENISONI)~~ MINI:S ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER ~ See instruction Description of Sampling Event: ,,-I _3=--ra __ Q_\N~o.X"_t_cr_~_h_l_ar_6_t6_o"'_'f'/I __ 2_0_1.2 ________________ ---J Location (well name): ,,-I -r.....;.....;:W_Ll--'--... O..;;.,.I'c. _________ ----' Sampler Name and initials: 1 -,-o.)11'1~r U;)J/1~/r1f- Field Sample ID 1 11N4~Ob-09112..D1'2.. Date and Time for Purging ,,-I --.;.'1/_lo.:-/..;..-':l.D;;;..;I;....-::z... _____ --' and Sampling (if different) V1//.201~ ~~-----------' Well Purging Equip Used: [!J]pump or [QJ bailer Well Pump (if other than Bennet) 1 6rtA"J.,-"Po.s Purging Method Used: 002 casings [QJ3 casings Sampling Event 1 Qv..tM-f~('b Ghloro--forM Prevo Well Sampled in Sampling Event I L-_~ __ ~_-_2f-______ --I pH Buffer 7.0 "-1_7_,0 ___ --' Specific Conductance 1....1 -:.,1'f...l..f1-'--___ .....I1 !!MHOS/ cm Depth to Water Before Purging 1 bGl .70 Conductance (avg) "--_?>..:o..-1oL-b_\ ________ --' pH Buffer 4.0 LLo Well Depth(O.Olft): ..... 1 -",1J_~...;..50 ___ --, Casing Volume (V) 4" well:1 j'H.5 1(·653h) 3" Well:l..... _D __ ---I.(.367h) pH of Water (avg) r......lIb=.3£.=..;::...-_____ .....I Well Water Temp. (avg) Ib.~ Redox Potential (Eh)1 3 5D Turbidity 1 q OJ Weather Condo I 'P ()I/~-.j clov.af Ext'l Amb. Temp. O( (prior sampling event) ..... 11_8..;...b __ --' Time I' 3113 Gal. Purged J....-::2_S __ ----' Time 1 I Gal. Purged I I Conductance 1 3'1 b 1 pH 1 6.3 b Conductance I I pH I I Temp.oC I )G."5 Temp.oC I 1 Redox Potential Eh (m V) I 2>3 0 Redox Potential Eh (mV) I 1 Turbidity (NTU) I ZJ03 Turbidity (NTU) I I Time I 01')..0 Gal. Purged Time 107Z3 1 Gal. Purged I I Conductance I ..... '.h_::l.._l_' __ --' pH I G:50 Conductance 13 "1:.07 I pH IG.Yo I Temp.oC 1 19.5(; Temp.oC I lY.s" 1 Redox Potential Eh (m V) I ..... '-I_L.\_~ __ ----' Redox Potential Eh (mV) I '-1~ I Turbidity (NTU) o Turbidity (NTU) 1 5:.1 1 White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) B~~r~ ...--------. Volume of Water Purged ... 1 _~ _____ .....I gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ...... 1 _10 ___ ....J Time to evacuate two casing volumes (2V) T=2V/Q= I 3.b3 I Number of casing volumes evacuated (if other than two) I '·3'1 If well evacuated to dryness, number of gallons evacuated 12.5 N arne of Certified Analytical Laboratory if Other Than Energy Labs .... 1 /1/._yA-_______ --I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs rx D 3x40 ml D rtJ HCL ~ D Nutrients t!!l D 100 ml D ~ H2SO4 ~ D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologics D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) 121 D Sample volume D M D ~ GhloflJe. If preservative is used, specify Type and Quantity of Preservative: Final Depth ... 1 ....:.~..;:..,_. b_6 ___ ....J Sample Time 0721 Comment ~ See instruction 1.. tr:\J1 \ on L.-l:,.. "'-~ 1 '2. --£ ~ -r" \ I' • t:>"'"L .... ,)-t-~ h .t I U/ t1 ~a I'.;;) T..... ",1 J.JO ~"'-t\n« ~f\/1I. V-G\fflt'\ ,I v,",vjT "'t()1 Vv.("~.e.., nA.('~<' ~~'1 <1\." 37 Y W"~e~ ",.1\ to..-6.. +6\-.... 1 of 2. "':""'-\-0 M~ ,,0 $G<.onJ..s, 'P ...... ~<l "".11 }( '::Jl. (,0 .... \<(' "" At>. r <. .. 11~ ,.., M~ "" it\, 5D"\1i n." \~ ? tAr kl~~, p",,~ ",,).) ... T n'l5. t.J} 51';1:-'I.} 13 LJ c. A(r"v~~ 01\ ~Itc:. ~t-0715. l~rjf}~" ~nJ, G",('rl'f) pr-esen1-1-0 Go)J-(.c7-~a.J1?ple~, D<!.p-tl, +0 W~+er ~ 6'1.E;;;, .s"'Mf')~ btAll~d, ~.j-07~1 i L~ SJ+C: A+ 07.2..5 TW4-0609-10-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 i····---·----·-------····------·--·------·-·------·-··---·-1 I OENISONr;)~~1 1 MINI:S ..--l FIELD DATA WORKSHEET FOR GROUNDWATER ~ See instruction WHITE MESA URANIUM MILL Description of Sampling Event: 1 3f"'JI Q""o..t=fer GhlorofbrY'1 ;<'012. Location (well name): ..... 1 :f-L-W_'1!..--...;:;.O_J _________ ----I Sampler Name and initials: 1 r(a.lln~ r-iJl>}/ J:J~?rH Field Sample ill Date and Time for Purging 1 ~ ,l and Sampling (if different) ..... 1 4...:.-J~J3;;;....:-;._~_O_)_2~ ____ __' ~Jl2./.2D12 Well Purging Equip Used: []!]pump or [gJ bailer Well Pump (if other than Bennet) '-16---'-ro;...;.Y\..;..;;t4--:....~ ____ ___' Purging Method Used: 00 2 casings [gJ3 casings Sampling Event I Q", ... r+erb::\ C~ \o,-..:t;; ... "" Prev. Well Sampled in Sampling E:entl ..... --.;l1~W_y;...;.-_]J ______ ___' pH Buffer 7.0 IL.o.--7..;...;....;;.' 0 ___ ---1 pH Buffer 4.0 Specific Conductance ..... 1 ....;.4~4~.!..-___ ----'1 !!MHOS/ cm Well Depth(O.Olft): 1 120.DD Depth to Water Before Purging 1 (;, g . ~ b Casing Volume (V) 4" well:1 3~. g~ 1(·653h) 3" Well: 6 (.367h) '--------' Conductance (avg) 1 SIt} L..-_=-~ ________ ~ pH of Water (avg) b .. 47 L..-~~ _________ ~ Well Water Temp. (avg) I )t-\.iY Redox Potential (Eh)1 ~U Turbidity ..... 1 _G}_I __ __' Weather Condo Ext'l Amb. Temp. O( (prior sampling event) ..... I.x<_l) __ ......I Time 1 J230 I Gal. Purged l51q I 5D 1 Time Gal. Purged Conductance 11.::), J'~i \ I pH 1 ',47 1 Conductance pH 1'----__ ---1 Temp.oC 11 4. 74 I Temp.oC Redox Potential Eh (mV) I Q.b~ I Redox Potential Eh (m V) ..... 1 ___ ___' Turbidity (NTU) I. '11 I Turbidity (NTU) Time 1 07D' I Gal. Purged I l) I Gal. Purged 0 r....-;... __ ---' Time I D7()~ Conductance I 1b{~ 1 pH 1 7 ·15 I Conductance IL--U)_3_1 __ ..... pH 1 7'.o~ Temp.oC I ':3. 3.5 I Temp.oC Redox Potential Eh (mV) I 2.L.F·~ I Redox Potential Eh (mV) I ;2..50 Turbidity (NTU) I g.~ I Turbidity (NTU) 1 (:1.3 White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) B~('e. ~J\-----' Volume of Water Purged .... 1 _5_u ____ --' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I'---Jo ___ --' T=2V/Q= I b.7b I Number of casing volumes evacuated (if other than two) 11197 If well evacuated to dryness, number of gallons evacuated Iso Name of Certified Analytical Laboratory if Other Than Energy Labs #/.4- ~------------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs ~ 0 3x40 ml 0 Tel HCL ~ 0 Nutrients 1!1 0 100 ml 0 IZI H2SO4 151 0 Heavy Metals 0 0 250 ml 0 0 HN03 D D All Other Non Radiologics D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) ~ D Sample volume D ~ D flg c,:h \ or; ~e, If preservative is used, specify Type and Quantity of Preservative: Final Depth 1-1 ....;..JHa.-q_.O_D ___ ....I Sample Time 6701Q Comment ~ See instruction A("r:vf!~ 6n ~a·~ 6..1-12.::tQ. -r ,,1\f\oe.,r o...f\ ~ G-o..f(~f\ l'(<6~t'\t..tor ?u .. r~e.. ?u.r~e. 1~j~n td-I ~:2.S plA.{'5~a we.lI +;'-r (}.. +"+,,,,\ f>~ .s Mifl""i-a;, 'H ... r~ej" Well ,ar~~ I,J"J-c.-W"¢ 111 ""rt((l' P\,\("B,-e,n~-e~ hJ-\2.30. L t;.fr ~/;te J-}~~~ Ard\l c.~ ot\. ~:t~ tf-+ 070 '--)~nn,r "'-V"lA G-~r"l1'\ p-re~e,.J. it> <:ol1e d-SlV'1f)e.s. De F+~ +0 lNo... .. h::·r bJ~S '~.1{1 b Gf, Lll J S CA}'V\r1~.s b~~ kd "'-+ ()7 Dc.., 1.. e.+t-S,+c.. 0..1-070'1 TW4 .. 0709-12-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 ~ See instruction I>ENISON~~~ WHITE MESA URANIUM MILL MINIES FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 31'")\ G)4v,iA,1"<r c.1110f'b::to(M ~o I~ Location (well name): ..... 1 _-r_~_~_-_O_g _________ ....... Sampler Name and initials: 1""1D..),Wlc:r Bb)J,j~!rH Field Sample ill Date and Time for Purging 1 8/Q..g/!)..Ol'2.. and Sampling (if different) 8/p·/17~Ol~ Well Purging Equip Used: [QJpump or [gJ bailer Well Pump (if other than Bennet) &fv..f\M~ Purging Method Used: 00 2 casings [gJ3 casings Sampling Event I CM",;:+<.('5 Gh 1 O,.~.f,;f rtl Prev. Well Sampled in Sampling Event 1L--J\r.) __ li_-_2._3 _____ --' pH Buffer 7.0 pH Buffer 4.0 Specific Conductance L-I _tf....:...q.:...;:1:....--__ ---I1 ~MHOS/ cm Well Depth(O.Olft): 1 l~.l>b Depth to Water Before Purging 1 bb 1 50 Casing Volume (V) 4" well:1 3g',~O 1(·653h) 3" Well: b (.367h) L--___ --I Conductance (avg) '--...;;:3:;;..;.2.....;7 ........ 1 _____ ----' pH of Water (avg) Well Water Temp. (avg) 1\5 .51] Redox Potential (Eh)lL-~7:.....;:::E::::"-_--I TurbiditYL-1 ...;...1 O..;...6~_--I Weather Condo IL..---_P._o.._r_~-=-_C_l {)_\A_J......::~~ ___ ---J Ext'l Amb. Temp. O( (prior sampling event)I&....;;;...:2.;...:.7_'D_----' Gal. Purged .sf) Time 11 y y go Gal. Purged Conductance 1 3~ 1'1 pH 1 ~,9;Z Conductance 3::27J pH 1 ?;,c!O Temp.oC Temp.oC Redox Potential Eh (m V) 76 Redox Potential Eh (mV) I ..... _7..:..;:~~_---I Turbidity (NTU) 10 \ Turbidity (NTU) Time ..... 1 ~l'i.1-Y.li..a9 ___ --, Gal. Purged 70 Time 119.5 C> Gal. Purged Conductance pH 1 (;,91 Conductance pH 1 '-'15 Temp. °C 1 15.DJ Temp.oC Redox Potential Eh (m V) 1 ..... _7._r5 __ ---I Redox Potential Eh (m V) ..... 1 _7....;;5~_---I Turbidity (NTU) Turbidity (NTU) JOD.) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1..-1 ~1 0=---__ ---1 T = 2V /Q = 1 7. bY I Number of casing volumes evacuated (if other than two) 1 b If well evacuated to dryness, number of gallons evacuated 1 b N arne of Certified Analytical Laboratory if Other Than Energy Labs 1...1 _~_/.""';~:""'-_____ ----I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs "[] D 3x40 ml D KI HCL ro D Nutrients "® D 100 ml D ~ H2SO4 19 D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) ~ D Sample volume D 'K1 D kJ CnlD\')~~ If preservative is used, specify Type and Quantity of Preservative: Final Depth 1 71, b5 Sample Time 1-.1 _O_1_:2!5 ___ .....I Comment ~ See instruction I\r"'i\le~ Of'. si+e 6.1-11-\3&. --(M~er "'''~ (fMr;" fCe.5.en1 ..fo'. pv-rqe _ f'v.0je h~"In oJ- \4 '-11... ?V\("~ed. '.f.)e\ \ -tDr "'--toto.\ of g tv1 ~Y'\~ ·h~ . .s. \.0",-+<:(" WAQ (}-1 ;1+\t;. ~ d,;rt I ?\Ar~~ en~e1 t1\i-lY5b Le+t Slte ~} J~55_ ~ Ar(i"e:~ 0(\ $:1-c. (1...1-O~\8. --r;..l'lncr o...r1d. (f&\rr;1) P('csC:f1t}o c.oJ/ec.'+ .. SC\f"1p)c.s, Oep-t~ 1-0 \A)tA..-kr \N~~ bbl~s?' Sa.(V1pl~.-5 b~:lt~ lA.-t oq~ .. Le.{1-.5J'+~ ~-t 01Q.S'. TW4-0808-28-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 r··-·----···-·······-·-··--···--·-··--·--····-I I OENISONI)~~1 1. MINES _ FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: l :s ('00 Qv...o..rt-er C\..l b'f'O'\(;(,rv1 ~o,~ ~ See instruction WHITE MESA URANIUM MILL Location (well name): L-1-r_W_'""_-_6_q _________ ---I Sampler Name and initials: I ~flnd" flo1},j~/11t Field Sample ID trw,., -O&f _ 0& 30 !2...61Q. Date and Time for Purging L-I g~J_~_!i.....;I.....;::z_O_J2. ____ _I and Sampling (if different) L-I &;;....;.!_3_b_I_:;1.._D--:..-.l2.. _____ --' Well Purging Equip Used: I]f]pump or [QJ bailer Well Pump (if other than Bennet) I G-rv." &;h;~ Purging Method Used: mJ2 casings [QJ3 casings Sampling Event IQ~,..[il Ch\orOF..ol'1 Prevo Well Sampled in Sampling Event 1L...."1""W __ L _\ -_O_~ ______ --I pH Buffer 7.0 7.0 pH Buffer 4.0 1.1.0 Specific Conductance 1L.--4'1_~ ____ ...J1 ~MHOS/ cm Well Depth(O.Olft): I 1 'AO ,be:, Depth to Water Before Purging I 59, S5 Casing Volume (V) 4" well:1 Y;2..73 1(·653h) 3" Well: 0 (.367h) L--___ --I Conductance (avg) ;l3~2... L--________ ~ pH of Water (avg) Well Water Temp. (avg) I )5.3D Redox Potential (Eh)L-1 _~.....;..<6.....Jl_----I Turbidity .... 1 _13_.5 __ --, Weather Condo Ext'l Amb. Temp. O( (prior sampling event) .... 1 M __ o _---' Time 1001> Gal. Purged Time I )OD 1 I Gal. Purged I 7(J I Conductance 1 23~?.... pH 1".75 Conductance I 2:5'2..J I pH Ib,71 I Temp.oC 1 15·~11 Temp.oC 11S.36 I Redox Potential Eh (mV) II,....;~;...;.;;...:...~.;...I __ --' Redox Potential Eh (m V) l 2.g0 I Turbidity (NTU) 1 131 Turbidity (NTU) 1)3:3 I Time 1 \OO~ Gal. Purged .... 1 ~=-O~ __ --' Time 1106.3 I Gal. Purged I ql) I Conductance 1 23;1.3 pH I C·II Conductance I .2.3;:LQ I pH I b f J] I Temp.oC 1 15.31 Temp.oC I IS.'3>D I Redox Potential Eh (m V) 278 1....----..;;... __ --1 Redox Potential Eh (mV) 11.75 I Turbidity (NTU) \3' Turbidity (NTU) 11QZS I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I'---'D ___ ---' T=2V/Q= 1 g.5Y 1 Number of casing volumes evacuated (if other than two) 1 0 If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs I ..... M_:lA-_______ ........ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs 1fl D 3x40 ml D ~ HCL 29 D Nutrients 1fl D 100 ml D 1t1 H2SO4 tJ D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) 1A1 D Sample volume D tJ D "t1 ["hlDr;~~ If preservative is used, specify Type and Quantity of Preservative: Final Depth 1-.1 7...;..D_ • ..;;;;.$..:.,J __ -.......I Sample Time ..... 1 _O_b_4_D __ ----' Comment ~ See instruction A(r-r\Jt:.~ 01'\ sii-~ "'+ 0'\ fl{) -r~(\ne.r ~n~ &~n": r1 b<e~err-Y ~r 'b""ro.e.. R \ ~ ~ . r '" ~ u..r~.fL i::I~n 0..-:) 0 <f 5lJ P\A.(£\~~ WeJI +o-r fA. +O+AJ of' 4' m,'\'\\A.t"c..s. w~+cr W'-.S ~ liH/e ca,'r+j, Pv..'-~~ ef)Jea t).1-ID03. Le+} .sl'f~ IJI.+ )007 Arr\"<=..~ 01\ ~'Tt: 1\:1-Ob~~ .. ~nt'\Gr" o..n~ &o.rr"n pre~n+ 70 Co)Je:d-scq~pJ~. Dep-Ji +0 wGt+t!r W~ 5L\.bO SdtMpks .b0\.:1~o..-r ObYO I l~*..srh:O\+ Of,lfY TW4-0908-29-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 1------------·] ;1.oE NM'.S.NO. ENs~.4 .4 1 . FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 3 ra Qv-.o..r+~r Gh lo,..o~~1'yV1 201'2. ~ See instruction WHITE MESA URANIUM MILL Location (well name): 1"'----r_w_L.J_-_JO _________ ----' Sampler Name and initials: I""" dt(\ ,,~r-+/0 OJ 'J4td frH Field Sample ID Date and Time for Purging 11..-~_7_Jl_/_~_1_2 ____ ____' and Sampling (if different) I ~J12.J-2C>1.2. Well Purging Equip Used: [IDpump or [QJ bailer Well Pump (if other than Bennet) 1 Grv,,,,a:(o.s Purging Method Used: ~2 casings [QJ3 casings Sampling Event I Qv.. ... r+Gr 1~ Gh )orof'orr>'l Prevo Well Sampled in Sampling Event 11..-11_W_t.t_-_, 8 ______ -..J pH Buffer 7.0 1-1 _7_"_0 ___ ---1 pH Buffer 4.0 4,6 Specific Conductance 1-1 _~_9~~ ____ ....I1 ~MHOS/ cm Well Depth(O.Olft): 11 \ \ • DD Depth to Water Before Purging 1155 I ~ 0 Casing Volume (V) 4" well:1 3f,.O,-\ IC.653h) 3" Well:l..-. _O ___ ....1.(.367h) Conductance (avg) L--_.2_Y..:..l.1-2 _____ ----' pH of Water (avg) Well Water Temp. (avg) I 15:31 Redox Potential (Eh)1 215 Turbidityl2Q. <. Weather Condo Ext'l Amb. Temp. O( (prior sampling event}II..-2.._3 _6 _---' Time 1 lDOi I Gal. Purged IY7.bD I Time Gal. Purged Conductance 1 :2.~)? I pH 1,·g1 I Conductance pH 1"'----__ --' Temp.oC I 1SI~' I Temp.oC Redox Potential Eh (mV) I ~l:; I Redox Potential Eh (m V) 1..-1 ___ ----' Turbidity (NTU) 1 :1.q,~ I Turbidity (NTU) Time 16707 1 Gal. Purged I 1) I Time 1..-1 0_7_1_0 __ --' Gal. Purged Conductance l 2.ql~ I pH I b .t16 1 Conductance I :rq 13 pH 1 <:;.:5) Temp.oC 11:5 .'19 I Temp.oC 1'5,73 Redox Potential Eh (m V) I :Lg~ I Redox Potential Eh (m V) 1..-1 !t_q_& __ ----' Turbidity (NTU) 1 7.ZJ I Turbidity (NTU) 7. g White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) B.e.+~'re. A-rte.r Volume of Water Purged Ll7.5D gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I 1D T=2V/Q= I 7.20 I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs 1-1 ..;.../\/.;....:/I.:....;~~ _____ ---I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs ~ 0 3x40 ml 0 ~ HCL ~ 0 Nutrients 1fl 0 100 ml 0 ~ H2SO4 ~ 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250 ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) ID 0 Sample volume 0 ~ 0 3 Chlor-l~je. If preservative is used, specify Type and Quantity of Preservative: Final Depth I 110. Db Sample Time 07D7 Comment ~ See instruction TW4-10 09-11-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) :-... _ .. _-_. __ .. __ .. __ ._---•.. -..•. -...... -... -.~ l'OENlsoNI)~~ MINES ~~-- Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 3ra Q v.,o..rtcr en 16rd'JrWl .2..0 1 ~ ~ See instruction Location (well name): 1-1-r"W __ \._'_-,_j _________ ----I Sampler Name and initials: l=r ;nner AolIIJ~/-nl Field Sample ID Date and Time for Purging 1 tot I , '2} ~O\ '2 and Sampling (if different) 1-1 ....!q:.;../_13~7:J.._D....;\:2,~ ____ ....J Well Purging Equip Used: rnJpump or @] bailer Well Pump (if other than Bennet) 1 Gr\AI'\LHoS Purging Method Used: ~2 casings @]3 casings Sampling Event I Q",,,, .-terfu G\-\ \o(,btt>rVVl Pre v . Well Sampled in Sampling Event 1L---r_\fJ_11_-_.2_' _____ ----' pH Buffer 7.0 7 .0 pH Buffer 4.0 q,o Specific Conductance 1-1 _1'tt...;.1 ___ ----'1 ~MHOS/ cm Well Depth(O.Olft): 1 lDO.oo Depth to Water Before Purging 1 S b . ~ 0 Casing Volume (V) 4" well:I.:2.15.lY IC.653h) 3" Well:L-. ..,;;;0 ___ ...... (.367h) Conductance (avg) 1 bD, '----~-----~ pH of Water (avg) Well Water Temp. (avg) 1 14 :;;10 Redox Potential (Eh)a..::;;;I2..S=-tf.:...-_ ..... Turbidity 1-1 7-'-=0 __ ....... Weather Condo Ext'l Amb. Temp. O( (prior sampling event) ..... I.-Z_l_" __ ....... Time &....1 _, D_15~_ ...... Gal. Purged lOU, Gal. Purged LjO a.......;..~_----' Time Conductance Ibo:t pH 1 ro.710 Conductance IbiD pH I ~·7~ Temp.oC Temp.oC Redox Potential Eh (m V) L--2._q_J __ ....J1 Redox Potential Eh (m V) 1...,;1 ~;...ff...&...;;.O __ ....J Turbidity (NTU) I c. 7, 1 I Turbidity (NTU) 70 Time 1 ...... 1...;;,.0..,;..11'--_---' Gal. Purged So Time t..-;I J...;..O ..... )&~_ ....... Gal. Purged Conductance \ 6\2.. pH Ib.7b Conductance 1 ..... \_'..;.;;;[5~_--' Temp.oC 14,31 Temp.oC 1 19.37 Redox Potential Eh (m V) 1...,;1 2;..;;;;;;...:.Q_O __ ....J Redox Potential Eh (m V)I t-,; ?)3~;.;;:8:.....-_ ....... Turbidity (NTU) 71 Turbidity (NTU) 173 White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1-1 _~_O ____ ---, gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1 )D T = 2V /Q = 1 -S. 6~ I Number of casing volumes evacuated (if other than two) I a If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs AI/A '----~---------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs ~ D 3x40 ml D f¥l HCL II D Nutrients ~ D 100 ml D ~ H2SO4 ~ D Heavy Metals D D 250ml D D HN03 D D All Other Non Radiologics D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) [J) D Sample volume D 159 D ~ ~ V\ \O'~~'G If preservative is used, specify Type and Quantity of Preservative: Final Depth ..... 1 '1_"....;.,....;;ct5=-__ ~ Sample Time Comment ~ See instruction A rrjve.a on ~;+e. 4.1-lOO!) • ...,....n~ ..... 0;",). G..rri" pt'eseYlt for ?v."~f-' p. ... r~~ b."~",,, fA} 10 IZ 'P",rfle~ """,11 ~. I--tot..) J; b r>'IinlA.+(';5, v.) ... -tGr vlc..5 \'VJo.~J}j Glo>J". P",r.je. OIl",J "'.} J OJt l A SJt'C,. 0..1-'O~ I ArTI''J-ed 01'\ ~I~e 0..+ DbS 1. -r~Y1n-(.r ~Y}J. GtArri1\ PPe-SeYl-3-+t> CoJ}e<:J .$~Mp)(!..s. Dep+h +0 tA.)fA.+er tN~ t;:,7.5$. ~1AfY)?1e.s. bt1\I'lc:a ~+ Ob'S7.. LG.+i-SI+e.. ~+ 07()D TW4-11 09-12-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL jr~~-~~~~~-~ ,_,~NI:S " . FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 1 3t'3\ Q""u"k. Cnloro=t~rM ~Ol~ Sampler Name ~ See instruction Location (well name): ..... 1 'T_\J_L\ ___ \~ ____________ ....... and initials: 1 ~nnc:"" goJ};J",~IrH Field Sample ID Date and Time for Purging 1 g / a.g/ ~D )~ and Sampling (if different) L.....\o8t..:..1.;;;..':l.~'1.:..J;;;...;:J..o~J~....=..-____ ...J Well Purging Equip Used: OOpump or [gJ bailer Well Pump (if other than Bennet) 1 &ruf\J..=\'~.s Purging Method Used: [QJ 2 casings [gJ3 casings Sampling Event 1 QV\().rh;d .. V\ chlDriJ'tofrr1 Prevo Well Sampled in Sampling Event I L-~ __ t1_-_0_0 _____ -...J pH Buffer 7.0 Specific Conductance ! L-_1.:,..1;....Jq ___ -...J! ~MHOS/ cm Depth to Water Before Purging ! 117.03 Conductance (avg) 1 O~O '--~~------~ pH Buffer 4.0 y.?) Well Depth(O.Olft): 1 101. SO Casing Volume (V) pH of Water (avg) 4" well:I .3S.Sb 1(.653h) 3" Well: 0 (.367h) L--~ __ ......I Well Water Temp. (avg) L-I _]5_' ._1_' _--' Redox Potential (Eh)!L-~..:..;5;;...1.. __ ......I Turbidity 1 ] y, bE Weather Condo 1L--.._-P_(}.._r_~_l t)~_C_\ O_\A_().......;~~ __ ---' Ext'l Amb. Temp. O( (prior sampling event)! ......... ~_l_l>_---' Time ..... 1 0_9_06 __ ----' Gal. Purged Time ! 090] Gal. Purged L-! _'_0 __ ...I Conductance pH !G.S4 Conductance L-11_0_7....;,.'1 _--, Temp.oC Temp.oC 115.15 Redox Potential Eh (mV) ..... 1 y...:...'_2 __ ....... 1 Yb2 Redox Potential Eh (m V) L-I q..;..,_O __ -...J Turbidity (NTU) Turbidity (NTU) Time l o40:l Gal. Purged 70 ......... _-_ ....... Time 10903 Gal. Purged L-I _3_o __ ...1 Conductance ..... 11_0_g_I __ ..... pH 1(;,59 Conductance logo pH 1 6; :38 Temp.oC I lSdl Temp.oC 115.07 Redox Potential Eh (m V) ..... 1 y...:,.50 ___ ....... Redox Potential Eh (m V) L-I 4_31_'1 __ ---' Turbidity (NTU) 1 ] 5, I Turbidity (NTU) 11$·3 White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1.-1 _1{) ___ ---' T = 2V/Q = I ry,1I I Number of casing volumes evacuated (if other than two) 10 If well evacuated to dryness, number of gallons evacuated 10 Name of Certified Analytical Laboratory if Other Than Energy Labs 1...1 #~'/_~ ______ ----I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs ~ D 3x40 ml D ~ HCL ~ D Nutrients fa D 100 ml D r:J H2SO4 ~ D Heavy Metals D D 250ml D D HN03 D D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) iCJ D Sample volume D '19 D .~ 6hlor'~ ~!. If preservative is used, specify Type and Quantity of Preservative: Final Depth L...;I 5;;.-'-_'_, 0...;.. . .....;~ __ ----I Sample Time I Db Y S Comment ~ See instruction TW4-12 08-28-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) f~~;;~;i)~-~ Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 31'a Q\;.;(f-cr Ghl{)r(;i:6fM ~OJ~ ~ See instruction Location (well name): L-1-r~'tJ_""'_-_13 __________ --I Sampler Name and initials: I1"*'AAf1Gf" »o));J~ ITa Field Sample ID Date and Time for Purging 1 g / :Lg/..2.0)~ and Sampling (if different) 8/.a.qI201~ ~~ _______ ---i Well Purging Equip Used: []IJpump or [QJ bailer Well Pump (if other than Bennet) 1-1 G-~('u._n_a_fl;:...:()::..;::s:....-___ --, Purging Method Used: 00 2 casings [QJ3 casings Sampling Event I Q,,-wTC.\i Ghlor~( r'l Prev. Well Sampled in Sampling Event 1,--'TW __ Y_-_1_~ _____ ---, pH Buffer 7.0 7.0 pH Buffer 4.0 '-I.D Specific Conductance L-I ..... jq_~'--___ ....II flMHOS/ cm Well Depth(O.O 1ft): 10-1 1_C>_{).._..5_0 __ ---i Depth to Water Before Purging 1 ~7.!2.b Casing Volume (V) 4" well:1 3 6.1 J 1(·653h) 3" Well: 0 (.367h) L.-...:::...-__ --' Conductance (avg) ~ '3 g '----------~ pH of Water (avg) 7.D~ Well Water Temp. (avg) 15, :S5 Redox Potential (Eh)1 Q...gg Turbidity 1 35.1; Weather Condo Ext'l Amb. Temp. O( (prior sampling event)a...;;.1 ~~o __ ....1 Time L-.1,_O_y*' __ --' Gal. Purged 10-1 _55 ___ --1 Time Gal. Purged Conductance pH 17. O~ Conductance pH IL--__ --' Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (m V) II--___ ....J Turbidity (NTU) Turbidity (NTU) Time la....;;o __ b_~_6 __ --I Gal. Purged Time 1 O~S" Gal. Purged 1"--__ ---' Conductance pH Conductance ~ b20 Temp.oC lb .. 86 Temp.oC Redox Potential Eh (mV) Redox Potential Eh (m V) 1...-1 _...::;.3-e2:=...Jo::..g---i Turbidity (NTU) o Turbidity (NTU) 0 White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) f~e-\-Dre Volume of Water Purged 11....-55 _____ --' ~ter gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = L-.I _1_0 __ ---' T=2V/Q= 1 7.~ I Number of casing volumes evacuated (if other than two) II.se?-. If well evacuated to dryness, number of gallons evacuated 1£5 N arne of Certified Analytical Laboratory if Other Than Energy Labs 1-1 _M_V,_:4-______ ----I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs &I 0 3x40 ml 0 rxI HCL ~ 0 Nutrients 121 0 100 ml 0 -00 H2SO4 ~ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) rn 0 Sample volume 0 ~ 0 ~ Ch\or~ae If preservati ve is used, specify Type and Quantity of Preservative: Final Depth ..... 1 _10_1_.0_Q ___ ....... Sample Time 0655 Comment ~ See instruction TW4-13 08-28-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 [.·.·· .. · .. ·.·-.·-··-----.----·.·· ... -·.· ... ··--.·.· .. ·-1 I.OENIS. oJ)jj.1 J MINES ~ FIELD DATA WORKSHEET FOR GROUNDWATER Description" of Sampling Event: 1 '3 ("'~ Q",o...,,'te.r Gh lor;fo{'yt') ;2.01:<" ~ See instruction WHITE MESA URANIUM MILL Location (well name): L-1_-f_\N_'-'_-_1'i....;.... ________ ---' Sampler Name and initials: 1 -r;.(lYler HoI FJII;O~/r1+ Field Sample ill Date and Time for Purging I g7~g7Q.Olr:J.... and Sampling (if different) L-I ..;;;.g~~_~.....!.4~/2_0...;..12~ ____ .....I Well Purging Equip Used: [1[]pump or [gJ bailer Well Pump (if other than Bennet) 1 G.".u(J Wo.s Purging Method Used: ~2 casings [gJ3 casings Sampling Event IQv.o.r-1-c::di1 Ch)o("0+6t"M Prevo Well Sampled in Sampling Event I L-_-r_W_t.{_-_1_3 ______ --I pH Buffer 7.0 L-I _-]_,_0 ___ ---1 Specific Conductance L-I _4.:....Jqa...:.~ ____ ....I1 ~MHOS/ cm Depth to Water Before Purging 1 2S b . SL-J Conductance (avg) 13.'1 L--~~~ _____ ~ pH Buffer 4.0 Y.D Well Depth(O.Olft): ...... 1 ...;..4 3_,O_D __ ---' Casing Volume (V) 4" Well:~Y-.-:2.-\ ---II <o653h) 3" Well:. 0 . (.367h) pH of Water (avg) 8, g J ~~~------....I Well Water Temp. (avg) 1 27, r1 Redox Potential (Eh)1 25c> Turbidity ...... 1 G~,5 __ .....I Weather Condo Ext'l Amb. Temp. O( (prior sampling event) .... 1 ~_b_o _-....I Time ...... 1 _12._\_3 __ --1 Gal. Purged 5 Time Gal. Purged Conductance pH I g.g) Conductance pH L-.I __ ---' Temp.oC I ~J.l1 Temp.oC Redox Potential Eh (m V) .... 1 2_'5_D __ -....I Redox Potential Eh (m V) .... 1 ____ ....I Turbidity (NTU) I b,S Turbidity (NTU) Time I 070b Gal. Purged Time 1 0707 Gal. Purged Conductance pH Conductance pH I , .. 46 I Temp.oC Temp.oC Redox Potential Eh (m V) Redox Potential Eh (mV) I 273 Turbidity (NTU) o Turbidity (NTU) Q White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ¥:>e;\-or c... V olume of Water Purged &....1 .....;.5~ ____ .....I gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = a....1 ---=.\=-0 __ ----' T=2V/Q= 1 · gy I Number of casing volumes evacuated (if other than two) 11.\6 If well evacuated to dryness, number of gallons evacuated Is N arne of Certified Analytical Laboratory if Other Than Energy Labs LLI M....JV,:....;../J_" ______ -' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs ~ D 3x40 ml D W HCL f!] D Nutrients 11:1 D 100 ml D ~ H2SO4 1K1 D Heavy Metals D D 250ml D D HN03 D D All Other Non Radiologics D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) l$J D Sample volume D 'ij;J D l1J {; h lO(·I~~ If preservati ve is used, specify " Type and Quantity of Preservative: Final Depth &....1 _q;....~_. O_t) ___ --' Sample Time 0706 Comment ~ See instruction TW4-14 08-28-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) r~~-N,so~ijl~,1 l,_MIN,_I:_S_' __ -" Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER orJi Q",~ ... fGr ch10("0+'0('('1 .2.012.. ~ See instruction Location (well name): ..... 1 _Pl_W_-_2fo __________ -----' Sampler Name and initials: r-rCl.nn" 8<3 J)jJaJlnJ Field Sample ID Date and Time for Purging .... 14..:...I_Y..;;,../_2_(:')_I'2.. _____ ----I and Sampling (if different) .... 1 A/._V~ ________ ----I Well Purging Equip Used: [![]pump or [QJ bailer Well Pump (if other than Bennet) IC61'):JJ~IAO\A..S Purging Method Used: [QJ2 casings [QJ3 casings Sampling Event IQv.o.4cr-..l::\ Ch I b rot<>n¥l Prevo Well Sampled in Sampling Event 1 .... 1W __ t./_-2_() ______ ----I pH Buffer 7.0 ..... 1_7_.o ___ ---' pH Buffer 4 .0 Specific Conductance .... 1 _q..;..~~~ ___ ---,I ~MHOS/ cm Well Depth(O.O 1ft): L.JI ):......22~.5_fJ __ ----' Depth to Water Before Purging 1 Sg. 7~ 4" well:1 ~ 1. ~ 1(·653h) 3" Well: b (.367h) 1...-___ --' Casing Volume (V) Conductance (avg) pH of Water (avg) Well Water Temp. (avg) 1 \5. yg, Redox Potential (Eh)1 17~ Turbidity .... 1 --..;;;0 __ ---' Weather Condo Ext'l Amb. Temp. O( (prior sampling event}I ..... .:<_g_· __ ...J Time ..... 1 \:_s'1tf--.;.... __ ..... Gal. Purged Time Gal. Purged Conductance I :)'13 g pH Conductance Temp.oC Temp.oC Redox Potential Eh (mV) )76 Redox Potential Eh (m V) ..... 1 ___ ---' Turbidity (NTU) o Turbidity (NTU) Time Gal. Purged Time Gal. Purged Conductance pH Conductance pH ..... I ___ -' Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (m V) .... 1 ___ ---' Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I lO.S T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) I e> If well evacuated to dryness, number of gallons evacuated 10 N arne of Certified Analytical Laboratory if Other Than Energy Labs .... 1 N_'/._'A _______ ----' Sample Taken Sample Vol (indieate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs lK1 0 3x40 ml 0 lJ HCL 1] 0 Nutrients 1tI 0 100 ml 0 "f] H2SO4 'lJ 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250 ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) lJ 0 Sample volume 0 m 0 ~ C h'Or-;J~ If preservative is used, specify Type and Quantity of Preservative: Final Depth &...;11;...0_3 _.'15..;.;;;;... __ ----' Sample Time \'550 Comment ~ See instruction MW-26 09-04-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ~ See instruction Location (well name): 1-1 _TVJ_~_-l_~ _________ --, Sampler Name and initials: --r;..nner" Ho 1) ,Jo..!VJ11 Field Sample ID Date and Time for Purging 1 8f.2.PJl.20 I Q.. and Sampling (if different) 1 ..... ~......;J;.....2_0...:.V_!2_o...&..)!2.. _____ --, Well Purging Equip Used: OOpump or @] bailer Well Pump (if other than Bennet) 1 G-n).od+oS Purging Method Used: ~2 casings @]3 casings Sampling Event IQv.o. ... fer"6 Col, \o~rM Prevo Well Sampled in Sampling Event II-T_W_L\_-_O_~ _____ --, pH Buffer 7.0 7.0 Specific Conductance 1-1 _q...;...q __ 1 ___ ---'IIlMHOS/ cm Depth to Water Before Purging 1 .5q. 3D Conductance (avg) a........:3:;..-'-4 ..... 7 ...... 1 ______ ___ pH Buffer 4.0 Well Depth(O.O1 ft): 1 JLj~. DO Casing Volume (V) 4" well:1 5". 0 0 I (.653h) 3" Well: ....... ....;,D __ ----I.(.367h) pH of Water (avg) ~.67 Well Water Temp. (avg) I 15, Y lj Redox Potential (Eh) 1L-...:..1 ~.;;;..6~_--I Turbidity 1 ..... _4 0 __ --' Weather Condo I 1-.. _S __ ~_~_n~~ ________________ ---I Ext'l Amb. Temp. O( (prior sampling event) ..... 1 ~ __ 'O _--, Time t3A5 Gal. Purged erb Time Gal. Purged Job Conductance I 3t1bg pH b,70 Conductance I '3l..fTT pH I f>.'~ Temp.oC 1 ]~,51 Temp.oC 1 15.41 Redox Potential Eh (mV) ''3>~ Redox Potential Eh (m V) 1-1 ..:...13.;;;..lj-6--_----' Turbidity (NTU) 1 gg.g Turbidity (NTU) Time 11327 Gal. Purged HD Time 1 J3~g' Gal. Purged 1-11,--~..;...D __ ...... Conductance 1 3~~1 pH b.hb Conductance 3Y75 Temp.oC 1 P:;:.,Cj3 Temp.oC Redox Potential Eh (mV) Redox Potential Eh (m V) I ........ J0..;..,3_0 __ --' Turbidity (NTU) Turbidity (NTU) 137.1 White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged l~O gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = L-I ---.;l_'D ___ --I T = 2V/Q = I 10. gC I Number of casing volumes evacuated (if other than two) 10 If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs .... 1 .....;M;.!.V,..:..;~:...-_____ ----I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs m D 3x40 ml D t1f HCL en D Nutrients m D 100 ml D rn H2SO4 ~ D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) rs D Sample volume D r!I D W 6hlD(,;~< If preservative is used, specifY Type and Quantity of Preservative: Final Depth I qg .53 Sample Time 1-1 O=--b_S_O __ ---' Comment ~ See instruction TW4-16 08-29-2013 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) I~;-;~i)~-~ FIELD DA~io=l~Ei~=DWATER Description oi -Sampling Event: 1 3 t"~ ex v 0..," t t:.,.r k LA. \ 0 (CJ.r 0 f"!IV\. ~D \ -:t ~ See instruction Location (well name): IMk) -'32>, Q 90S:;:to ~ h ~t..V-:32.. Field Sample ill 1 M LJ ~ 6.2< 09 05 2=~ I ~ Date and Time for Purging 1 09 10 (; l:l 0) 2. Well Purging Equip Used: [][]pump or @] bailer Sampler Name and initials: 1 6o..f'f" ill\. Pq.....lVV\lt!..\ I 6 P and Sampling (if different) Well Pump (if other than Bennet) QED Purging Method Used: [][]2 casings @]3 casings Sampling Event I Q" ..... + e:.r \ t £.l.. \ 0'-0 .. 0 ..... >M. Prev 0 Well Sampled in Sampling Event I -rw 'i ~ Cl i pH Buffer 7.0 7 .. 6 Specific Conductance L-I -...:.q_Cf.:-CJ"':"'-__ .....I1 flMHOS/ cm Depth to Water Before Purging 1 7 Y # GIS 1 Conductance (avg) '---_3_g'--3;;;;;.....;:;b'--___ ~ pH Buffer 4.0 LJ" b Well Depth(O.Olft): 1 130 .,Ib Casing Volume (V) 4" well:~_3~6-r-J _6 --1I Co653h) 3" Well:. 25 ,c367h) pH of Water (avg) L..-1 ----J.601U1;~S:;;...:g~ ___ _____I Well Water Temp. (avg) 1 JEt 7 g Redox Potential (Eh)1 J b z...J 1 Turbidity I 7. J Weather Condo I ..s V v'\. 0/'--Y Time lY:S.5 Gal. Purged Conductance pH Temp. °C I £ / 7 b 1 Redox Potential Eh (m V) I 1 I> I Turbidity (NTU) I 6, q Time 1 1 Y37 Gal. Purged Conductance 1 3 g ?--£; 1 pH Temp.oC 1 £ .. 73 1 Redox Potential Eh (mV) 1 l66 Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 73, 11J 1 6,57 Ext'l Amb. Temp. O( (prior sampling event)1 2(:) 0 Time Gal. Purged Conductance Temp.oC Redox Potential Eh (m V) I 1 6 q Turbidity (NTU) Time 11Y38 Gal. Purged 733yl Conductance 3857 1 pH 1 6,57 1 Temp.oC 15. q Y 1 Redox Potential Eh (m V) 1 I ~ 7 Turbidity (NTU) 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0. I gallon{s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60= I , ~17 Time to evacuate two casing volumes (2V) T=2V/Q= I Z,iS7 .. q3 I Number of casing volumes evacuated (if other than two) AlA If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs ,/V A ~~------------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs ~ 0 3x40 ml 0 ~ HCL ~ 0 Nutrients ~ 0 100 ml 0 ~ H2SO4 ~ 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) ~ 0 Sample volume 0 ~ 0 ~ L..,l.A ~O r-; ~~ If preservative is used, specify Type and Quantity of Preservative: Final Depth I 7q .. Q3 Sample Time 13YtJ Comment ~ See instruction MW-32 09-05-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2of2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) r-----------------1 jl.OENISONl)jjl MINI:S ~_ . __ .....1 Description of Sampling Event: ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER 1 '3<'tA Qv...o..f"'te(" G'h \orCfFo( M 2.6'2. ~ See instruction Location (well name): ,-I 'T_w_~_-_l_g _________ ----I Sampler Name and initials: 1 :::::r,.,VIn (!,.-t1 6 1hJd'I.!1 1ft-} Field Sample ID 1 TW '-\ -\ g _ oq , 1 'J..D 1 '2.. Date and Time for Purging L..1_1;..../_10;...;.~-='2=-O...;.1_~~ ___ ----J and Sampling (if different) t:tll1/~Dl'J.. ~~-------~ Well Purging Equip Used: [QJpump or [QJ bailer Well Pump (if other than Bennet) 1 6-f'lAYl~+o.s Purging Method Used: [![]2 casings [QJ3 casings Sampling Event I Q", ... .-k8 G\' \o,.(;ForfIIJ Prev. Well Sampled in Sampling Event 1 ..... ""_W_t..:_~_-_D_L5 _____ ~ pH Buffer 7.0 1,0 pH Buffer 4.0 \..).0 Specific Conductance 1-1 _'1_1....;.~ ___ ----'1 !!MHOS/ cm Well Depth(O.Olft): I )37.50 Depth to Water Before Purging I 5-'. 2.0 Casing Volume (V) 4" well:I .5::l·'1~ 1(·653h) 3" Well: 0 (.367h) "'---"-----' Conductance (avg) :l.O"1':;' '------------------~ pH of Water (avg) ,. q,b '--~------------~ Well Water Temp. (avg) 1 '!>./~ Redox Potential (Eh)1 30'1 Turbidity .... 1 ~_O£,. __ ...... WeatherCond. I 'P(,<.~ L\Dv-~~ Ext'l Amb. Temp. O( (prior sampling event)I .... :A_7_O_----I 80 Gal. Purged Time 1307 Time 1 J30g Gal. Purged q 0 ""--------I Conductance pH 6.59 Conductance Temp.oC 11S.73 Temp.oC Redox Potential Eh (m V) 31 b t....-..,;;;~ __ ...... Redox Potential Eh (m V) 1......:3=-....;11:.--_----1 Turbidity (NTU) I 'l-Oi Turbidity (NTU) 201 Time '-'II )-=3~O;.....<1.:....-_--, Gal. Purged )00 Time IoL:D3::.::;,.J...;;,D __ --' Gal. Purged po Conductance tLO 73 Conductance ::tog \ pH I '·93 Temp.oC \5. [3 Temp.oC Redox Potential Eh (m V) 3 0", a.......:::; ___ ...... Redox Potential Eh (m V) 1 ..... 3_0_s __ ----I Turbidity (NTU) I ~Ot) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged J } 0 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 =1 L.-~l..:;...D __ -----' T = 2V /Q = I '0, l..18 I Number of casing volumes evacuated (if other than two) 1 0 If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs 11..--;V._1J_~ ______ ----I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs ~ 0 3x40 ml 0 B HCL ttl 0 Nutrients r.B 0 100 ml 0 lJJ H2SO4 rn 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) ~ 0 Sample volume 0 ~ 0 $I Gh\()'(\~~ If preservative is used, specify Type and Quantity of Preservative: Final Depth l.:s 1. ~s Sample Time &....1 D_7_47 ___ --I Comment ~ See instruction An' ;\le c\ 01\ ~ ;t l: ",--Y 1 '-j5S. I ... " n er "' .... a & Mr ; n pn~.s c,,} -h,( ? ",r~ -e. 'P "' .. ~<. b e ~().T\ /ivt J~54. ?lA<~Ga VJ~\\ fc,r tJf... +o+~l 0+ )} W)inu.-Te.s. \J.)o..-hr-V-)~ MlA.("~ \...)li-h SO}n1e s~",J P,,~;6\<?\ ?v..r~< O1ael ~ )31D ~ L(!~ ~;1-'(. ~t ~3'~ A1"f,'\)etl on s\~h:. tA.t D11..]0. ~n(\-c:.r AnA 6-(A{'dn pf"~.s.e~ +0 GOI}u.1-~IifMp}CS. D~pt~ fo ~Q.+G" w~s. 57.2.1 ~AMp\-!.~ b~,'\etX, 0.." 07t41 TW4-18 09-10-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) rOE;~;E;ij1~l FIELD DA~~ioal~~Ji~:U~DWATER ~ See instruction Description of Sampling Event: I 3 ",J< U!?vwr+GJr ?iA.\c>-ro -Yof"'VV' ~012 Location (well name): IL..-.:..T_W_\1.....:.-o-J....:..l--lqi..--________ ---J Sampler Name and initials: I ~GoUt""'lV'\, P~V'--VGlr' Z &p Field Sample ID Date and Time for Purging I C) Cf /6 S I '201 ~ and Sampling (if different) Well Purging Equip Used: OOpump or [QJ bailer Well Pump (if other than Bennet) Purging Method Used: [QJ2 casings [QJ3 casings Sampling Event I"", v ""r' t ",r'\ j L..l... \ Dr'" ~ 0 rd Prev. Well Sampled in Sampling Event I /':Ai W ..J 3 2 pH Buffer 7.0 pH Buffer 4.0 Specific Conductance L-I _.....;q~9..!...-~.J..-_----oI1 ~MHOS/ cm Well Depth(O.Olft): Depth to Water Before Purging I 15 Cf" 7 () I Casing Volume (V) 4" well:1 1j~J 6L-l 1(·653h) 3" Well: (.367h) L--~-",,-_--' Conductance (avg) '---_2~8~1..-.::6~ ___ ---I pH of Water (avg) 6",16 I Well Water Temp. (avg) I 15, L15 Redox Potential (Eh)1 :3 ~ ~ I Turbidity I 6 Weather Condo 1L--_5 __ v_V"-_IAI_i..&..-_______ ---J Ext'l Amb. Temp. O( (prior sampling event)1 :22 Time ID35 Gal. Purged C) Time Gal. Purged Conductance pH $","fb Conductance pHI Temp.oC I ,SI( yE Temp.oC Redox Potential Eh (mV) I 3 22 Redox Potential Eh (mV) I Turbidity (NTU) I 0 Turbidity (NTU) Time Gal. Purged Time Gal. Purged Conductance pH Conductance pHI Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (mV) I Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I lL( v 6 Time to evacuate two casing volumes (2V) T=2V/Q= I c> I Number of casing volumes evacuated (if other than two) iliA If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs AlA Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs !Sa' 0 3x40 ml 0 rii HCL ~ 0 Nutrients 5l 0 100 ml 0 rE H2SO4 0J 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) 15l 0 Sample volume 0 [S! 0 Q C ~\ or-.~~u If preservati ve is used, specify Type and Quantity of Preservative: Final Depth I 6$ ttl :3~ Sample Time lOYD See instruction Comment Arr-·'vt,..~ ~V\-$'-+t/ ~-r ~CS:30 .. t"c,...Kr-~V'-" ~~ \&".MNc.r fru£f:#'Vt-{3C?r" ~~(,,;~ ~l.I~""+' Pc...rtNJIV\.~.yz::..'.s t.Vc..rc.., +&u~~ c....i--1 "Z,.£"i ..5~VV\lf~t,;S Wc.r'~ t.oll,",v~~ ~{. I b t.J\O... W ~r~ ~Od t-~~ c..~t;..VV-.. /..t,fJ i' 5, .. t e. ~~ ~O t.1~ .. TW4-19 09-05-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ~ See instruction Location (well name): 1L--'T_W_Ll_-_A_D _________ ---' Sampler Name and initials: I~nn(,r JO.}oJ},J \'1 /TH Field Sample ID Date and Time for Purging ..... 1 q..;.:/_Y..;,.I_:2._0_1 _L.~ ____ __' and Sampling (if different) ..... 1 ~--=-VA ________ ---I Well Purging Equip Used: 1'tJ Ipump or [gJ bailer Well Pump (if other than Bennet) k:.o,J/1"J lA ou...S Purging Method Used: [gJ2 casings [gJ3 casings Sampling Event 1Qv.tJ.f-\-erb Ghloro-torrvl Prevo Well Sampled in Sampling Event I ..... _T1_W_LJ_-_-2_7 _____ --I pH Buffer 7.0 ..... 1 _7_,_D ___ -----I pH Buffer 4.0 '-/. t) Specific Conductance ..... 11_q_q ________ 1 ~MHOS/ cm Well Depth(O.O 1 ft): 1.......,;..1 D....;:6;....' D;;;.,.;;O"---_---' Depth to Water Before Purging I 5b.3.5 4" well:13;l,.}1Z. ·1(·653h) 3" Well: 0 (.367h) 1.-___ --1 Casing Volume (V) Conductance (avg) ,--Y...:..3~!2..~O ______ __, pH of Water (avg) ..... 1 _b_.5_7 ______ __' Well Water Temp. (avg) 11.03 Redox Potential (Eh)1 ~ '4:l. TurbiditY ..... I .2--,,·~ __ ...... Weather Condo Ext'l Amb. Temp. °C (prior sampling event) ..... 1 ~_g_o __ ...... Time ..... l l_3_~_Y __ ...... Gal. Purged I b I '---------' Time Gal. Purged Conductance I L13::;.l) pH I G.57 Conductance pH I L-__ ----' Temp.oC Temp.oC Redox Potential Eh (mV) 2..'-12-L--,;;;.,...;.. __ ---' Redox Potential Eh (mV) 1-1 ____ ....I Turbidity (NTU) 1 2. .21 Turbidity (NTU) Time Gal. Purged Time Gal. Purged Conductance pH Conductance pH ..... I ___ ...... Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (mV) 1-1 ____ ....1 Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged o gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I 10..5 T=2V/Q= I D I Number of casing volumes evacuated (if other than two) 1 0 If well evacuated to dryness, number of gallons evacuated I ~ Name of Certified Analytical Laboratory if Other Than Energy Labs ,tV/A ~----------------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs l!1 D 3x40 ml D i!1 HCL ~ D Nutrients 00 D 100 ml D ~ H2SO4 l!j D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) rn D Sample volume D ~ D 19 0h \or; je If preservative is used, specify Type and Quantity of Preservative: Final Depth 1-1 4....;.;$;.....7_1 __ ---' Sample Time 1-1 _13_3.5 ____ -1 Comment ~ See instruction Arr;veJ. on s.i·h~ o.-t IQ8. l"l'lnt'r-~"J. GtJt.rr-j", pr~sc1'rr70 coJlec.7 .$4mp}c.5. S"MP""< coJJ",,*,,,d ... J 13:35. \.0<t+cr 1N4S """.st,!,j Cl",,>.r. \.. d+-~ ;1-" ,,-1-J3YD TW4-20 09-04-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL 1~~;s9Pl~ FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: '?J-r-A Q\AO.rfGJ" Gh 1 orof0r!V} 2.al~ ~ See instruction Location (well name): .... 1 _~_w_L\_·:l.-.:-.1 _________ --' Sampler Name and initials: I~nnt:\ HolhJ\~Ir-lt Field Sample ID 1 ~tv>Jbl,":2J::-~·f,}4.t:~t7::t71.:;?t;: \ ITt"u J I = ~ 1 .. 0 q 1 ;t:2- ~-----"----------'_r'v\.)~ ... ;2.1-o9l32P\~ Date and Time for Purging 1 tl/n/::?o!'2_ \ 'Gt/l;'-/;'Ol~ and Sampling (if different) tjh~:t/2/.q:;t .. ' ~---~-------' Well Purging Equip Used: l-m Ipump or @] bailer Well Pump (if other than Bennet) 1 (fruYla~s Purging Method Used: 00 2 casings @]3 casings Sampling Event 1 Qv...G\...t.c.fb C h \or~("M Prevo Well Sampled in Sampling Event I .... _'T'W __ t1_ ..... _:x2. ______ --' pH Buffer 7.0 7.0 pH Buffer 4.0 Specific Conductance L-I --'4;....;.44~ ___ .... 1 ~MHOS/ cm Well Depth(O.Olft): I /.2..1. o?> Depth to Water Before Purging 1 5'-\, L\ ~ Casing Volume (V) 4" well:1 Y3,'-\7 1(·653h) 3" Well: a (.367h) '---___ --I Conductance (avg) 350 \ '---~~------------~ pH of Water (avg) Well Water Temp. (avg) I IS . ~ \ Redox Potential (Eh)1 L-~_4q __ --, Turbidity 1 J1, LJ~ 1 J 7 t L/ ~ Weather Condo Time I ...... D_&_:l_7 __ --' Gal. Purged ...... 1 _b_O __ ---' Conductance Temp.oC Redox Potential Eh (m V) .2C;1 Turbidity (NTU) I 1(;).9 Time I 0 8.2,G} Gal. Purged g l) '---~----I Conductance Temp.oC Redox Potential Eh (m V) L...,;I :2.~qq~_---I Turbidity (NTU) HS.O White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event) .... ' _:L_,_l>_----' Time 1 Og~g Gal. Purged 76 '---__ ---I Conductance I ~4'" 1 Temp.oC I 15 .QI Redox Potential Eh (m V) L-I _~--,q:....64 __ .... Turbidity (NTU) Time I Og'30 Conductance I :353\ Temp.oC I [5. ~ I \1.0 Gal. Purged I ....... CJ_D __ ----' pH I 6. ttl Redox Potential Eh (m V) 1L-2:;_H't __ ---' Turbidity (NTU) 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = lL..........;l~D ___ --J Time to evacuate two casing volumes (2V) T = 2V /Q = I g. f}~ I Number of casing volumes evacuated (if other than two) I b If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs I ..... N_/_"1 ______ ---J Sample Taken Sample Vol (indieate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs ~ 0 3x40 ml 0 1lI HCL WI, Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specify) C h\O~~~e. Final Depth IL..--b q_.I_J __ ----' Comment A~"riveA 01\ ~Ii-c: ~-t 0 g 17 Pv..r~~J. v.)e.\\ ~or (k +ot~' L.e.tt s ;t-G. C\~ og3l..\ ~ 0 100 ml 0 ~ H2SO4 ~ 0 0 250 ml 0 0 HN03 0 0 0 250ml 0 0 No Preserv. 0 0 0 1,000 ml 0 0 HN03 0 'tB 0 Sample volume 0 ~ 0 If preservative is used, specify Type and Quantity of Preservative: Sample Time ..... 1 _6_b....:':l5=-__ ..... ~ See instruction -ro..n,.,~r a.nJ. (ivaN"';' f(,GSc.,·)J +0"'" furce . P~t~e .b~qn cd-0 8~ / 0+ q ~;r1lA+es. lJ.)o:T~r wo.s c.lco.('.. f-\A(~<: cnde~ A..t 0830. N 0 0 0 0 0 00 Ard'le.l Of\ site. ik.t 6.b3~ .--rA.t'\1\e(" ~na G-tA.r6f\ rre..sey1} +6 Ge> llt:.c+ ~tAMple~, DGP-tl, -to !Nc\'1Gr w~s 5't30, S~Mp1cs bG\;le~ 6-.1-06'"1 S. l-ef+ srte. ~t-()'~C/ TW4-21 09-12-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ~;;;~1j1~ FIELD DA~~~~::l~~Ei~:O~~WATER Description of Sampling Event: 1.3 r a Q V. ~ .... fGr Gh \ ()rD'Fof'yv'l ~DJ.2. ~ See instruction Location (well name): 11--r_W_t1_-_:L_2. __________ --' Sampler Name and initials: Fi:"n<:r J.} ol1;J"'d~ Field Sample ID Date and Time for Purging I",,--Gl_I_l_1 /_:l.._D_l_~ ____ ----, and Sampling (if different) qllQI:.2.o}~ ""------------~ Well Purging Equip Used: [£[]pump or [gJ bailer Well Pump (if other than Bennet) I Z;:r'\At1tJJD~ Purging Method Used: [][] 2 casings [gJ3 casings Sampling Event 1 Q",,~4Gf"1~ Chlo-r~l"'M Prevo Well Sampled in Sampling Event I I--r_W_t1_-_1_0 ______ ---I pH Buffer 7.0 7,0 Specific Conductance 1-1 _q ........ q_~ ____ ....I1 !!MHOS/ cm Depth to Water Before Purging 1 53. 0':2.. Conductance (avg) 52>;2.3 L--~ _____________ ~ pH Buffer 4.0 Well Depth(O.Olft): 1 113150 Casing Volume (V) pH of Water (avg) 4" well:1 :3'1.'1'1 I (.653h) 3" Well:L-. _() __ ~.(.367h) Well Water Temp. (avg) 115.$4 Redox Potential (Eh)I,--:;l:._~_l _~ Turbidity ..... 1 0 ___ --' WeatherCond. I 'PM 1\j OOu.~'2 Ext'l Amb. Temp. °C (prior sampling event)l&... ~_3_b _--, Time Gal. Purged Time 1 )2;2..~ Gal. Purged I I-'_6 __ ...... Conductance pH Conductance 1 5~ Temp.oC Temp.oC 1 15 .89 Redox Potential Eh (mV) Redox Potential Eh (m V) 11-.-.:2.._7_1 __ ...... Turbidity (NTU) Turbidity (NTU) Time 1 ~lf·;;':!.fl\ Gal. Purged 70 "I Time l-l'Q.:2 .. ·t~, I Gal. Purged 1 80 .. 07~ ,.........,........,.._---. Conductance I ' h bS pH ,--7_, _0_<3 __ --' 07~'4 Conductance ..... 1 l"""G""-l"Dr----.. pH 1 7, O~ Temp. °C 115 . n Temp.oC I 15, ILl Redox Potential Eh (m V) ..... 1 ~_8-:5~_--, Redox Potential Eh (m V) &...1 _::[_8_" __ ...... Turbidity (NTU) I " b Turbidity (NTU) 1 1. 8 White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V 1 fW ~~d f'~~""n~", -----. o ume 0 ater Purge I ...... ...;;,L_ .. ,L_. '" _' ___ ---I gallon(s) b 7.EI:> Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1...-1 _'0 ___ ---, Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V /Q = I,. g~ I I..Q-1.70 L..-I-'L~' I _----II Co I, 5b N arne of Certified Analytical Laboratory if Other Than Energy Labs L-I _/lJ._~_~ ______ ----, Sample Taken Sample Vol (indieate Filtered Preservative Added Type of Sample if other than as Preservati ve Type y N specified below) Y N Y N VOCs ~ D 3x40 ml D ~ HCL !J D Nutrients ~ D 100 ml D ~ H2SO4 ~ D Heavy Metals D D 250ml D D HN03 D D All Other Non Radiologies D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) ~ D Sample volume D fB D ~ Ch)C>~;~C If preservative is used, specify Type and Quantity of Preservative: Final Depth I ll~.oc> Sample Time 07Z1... Comment ~ See instruction TW4-22 09-11-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 OENISONI).4~ ~ See instruction WHITE MESA URANIUM MILL MINES FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I 3("3\ Qv..~f4'e('" Ch1orM"'c,fM ~ 12. Location (well name): 1-1-r_w_'--\~-.2.3-=-_________ --I Sampler Name and initials: I ~rlfle'" Hol1;J~111:t Field Sample ill Date and Time for Purging I g/:;...g/ao\'2.. and Sampling (if different) 5/~~ 7 ~O\2.. Well Purging Equip Used: [QJpump or @] bailer Well Pump (if other than Bennet) I I-.loLG-....;..r..;;..;,\)...1\.....;..A;,..:.;fC~o.S=-___ ----J Purging Method Used: I][] 2 casings @]3 casings Sampling Event I Q""'c').("1-cr},) (.),,It><o-tOrrA Prevo Well Sampled in Sampling Event I ..... _"-"-'_l _W_'1_-_I~ _____ ---I pH Buffer 7.0 pH Buffer 4.0 Specific Conductance 1-1 _4_q...:..~ ___ ---II ~MHOS/ cm Well Depth(O.Olft): I liL\.Db Depth to Water Before Purging I b L1. Sb Casing Volume (V) 4" well:1 ~~.~8 1(·653h) 3" Well:L-. _O ___ --I.(.367h) Conductance (avg) 3"L\..3 L--~_~ _____ ~ pH of Water (avg) Well Water Temp. (avg) I 15.0'D Redox Potential (Eh) I~) ~ ___ t)=--_---I TurbiditYIL.=5::"-~--"';';;;"'_---I Weather Condo Time ..... 1' ___ .3_0_~ __ ..... Conductance Gal. Purged 1-1 _y....:-O __ ---I pH I C).So Temp.oC 1 '5,ob Redox Potential Eh (mV) ..... 111.-1_li __ ----I Turbidity (NTU) 1331 Time 1 \30$ Gal. Purged bO ........... '-"---_--1 Conductance 1 3> '9 tJ pH 1 G,9'3 Temp.oC Redox Potential Eh (m V) 1:21 Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Ext'l Amb. Temp. O( (prior sampling event}1 ~Cr.,"b Time 1L-'_3_D_y _---I Gal. Purged 5 D 1...--__ ----1 Conductance Temp.oC 15,0 \ Redox Potential Eh (m V) ..... 1 _1 !l:_D __ ----' Turbidity (NTU) Time 1 1 3D b Gal. Purged ..... 1 ' ____ D __ ---I Conductance 1 3bY): pH 1 6. ~ , Temp.oC Redox Potential Eh (m V) IL--,!Z_I __ ---I Turbidity (NTU) 1 3;;(/ 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (CAP) V olume of Water Purged 10 gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I,---'~t) ___ --I T=2V/Q= I b.tt5 I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated o Name of Certified Analytical Laboratory if Other Than Energy Labs tV/A ~-----------------I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs () D 3x40 ml D ~ HCL ~ Nutrients rfj D 100 ml D [] H2SO4 W Heavy Metals D D 250 ml D D HN03 D All Other Non Radiologics D D 250ml D D No Preserv. D Gross Alpha D D 1,000 ml D D HN03 D Other (specify) 1\\1 D Sample volume D 111 D Chloe; ~~ If preservative is used, specify Type and Quantity of Preservative: Final Depth I g D . .5b Sample Time 64)3 Comment ~ See instruction Arr:\le& 0\'\ ~:+e ... + );t5b. ~nner "'",}. G-o..rr:'" F' ... e~c"t +';r l'","'~e. P"'r~.., he(j"''' ... t 1::l.5'f ?v..('f)"ed ~~11 ~'(" fk. 4--0+011 o~ 7 m;t'\""'+e.S. \A)4c.r nA.~ <J."., ';(1.l,t r \ ~ t ~ ~ 0 o...n ~ e c-o Or 'TO i . ? \kr~~ er\k~ ~ t 1~ DC:. I Le&1 ~)lG 0 }~ 1 D ~ Arr;\le~ 0(\ s;1--e. o;.t Ca.D7. --r;.flY'er ll.f'ltA Cro.(r.'n pieSen+ 1-0 co/lee.} .sa.MpJe s Dep+h 1-0 wG\.~~r \,.)o..s bY. 55 .s tN""lf1t!S ~ere.. bO\.;)e~ ~1-0'113. L e.+t ~ ite ~-t 0 Gf 17 TW4-23 08-28-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D ~ 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ~ See instruction Location (well name): 1 I.-_-r_w--.....;'-1_-_.2!.....;y~ ________ --I Sampler Name and initials: I ~Y1nv OJJ"Jh'J~ In~ Field Sample ID Date and Time for Purging I g/ ~1/;2.0J:2 and Sampling (if different) gJ3D/~J~ Well Purging Equip Used: [][]pump or [gJ bailer Well Pump (if other than Bennet) 1 (;..,.",n J :f~.s Purging Method Used: 002 casings [gJ3 casings Sampling Event I Q", .. r+er G\ Gh 1 orOBo", Prevo Well Sampled in Sampling Event 1'-----r_W_Y_-l_~ _____ ___' pH Buffer 7.0 7.() pH Buffer 4.0 Specific Conductance 1.-1 --:.~_1_~ ___ --'IIlMHOS/ cm Well Depth(O.Olft): 1 11..2,50 Depth to Water Before Purging 15'1. bY Casing Volume (V) 4" well:I ;:'].1 g I (.653h) 3" Well:L-. _'b __ --I,C.367h) Conductance (avg) pH of Water (avg) Well Water Temp. (avg) 1 15 .SL Redox Potential (Eh)1 ~~ Turbidityl~5_. D __ --' ~38 Weather Condo I'---__ S_""_(\_l'\_il ________ ___' Ext'J Amb. Temp. O( (prior sampling event)I~~_~_l) _---I Time 1 P-lD.s Gal. Purged Conductance l'---q3_'1_1_----I Temp.oC Redox Potential Eh (mV) Turbidity (NTU) Time ~I _1 ~,,-D-:.7 __ --, Conductance Temp.oC )5,510 ?..97 Gal. Purged L.o-1 _7 ..... ?l __ ----' pH I b·G~ Redox Potential Eh (mV) I .?.'3S Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Time 11YOb Gal. Purged 66 L--__ ---' Conductance 1 'r~b7 Temp.oC I 1.5. sZ) Redox Potential Eh (mV) I :;...y=t Turbidity (NTU) 5.D Time L-JI IL.....ILj..::;,.OJ..l,cs_---I Gal. Purged Conductance I qSq:s . I pH I b·71 Temp. °C I }5 .SL) Redox Potential Eh (mV) I a..3D Turbidity (NTU) 19.7 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 36 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 =1 L.-_]_0 __ ----1 Time to evacuate two casing volumes (2V) T= 2V/Q = I 7.55 I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated 10 Name of Certified Analytical Laboratory if Other Than Energy Labs ..... 1 _/J._y._~ ______ ----, Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y VOCs ~ 0 3x40 ml 0 "!J HCL "flJ Nutrients p 0 100 ml 0 'tJ H2SO4 't:!J Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologics 0 0 250 ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) lJ 0 Sample volume 0 '!;;] 0 Ch\o~\ac. If preservative is used, specify Type and Quantity of Preservative: Final Depth I bl , Y ~ Sample Time 07l>b Comment ~ See instruction Arrl\l~~ 01\ s:+c. ~~ 135b ~nt\er c1J)a G-~("(;n rcesct)-t -tor ?u,...~e. Pu..(""~e. :b~~1) "\.+ }1.f6O,. Pv.(~e~ \0cll +Or (io.. +0+",,1 of' g yY)jY}vJes, woJe(" Wb..S c.1-eo.~_ Pv.('~~ ~Y}J.t:~ 6-.1-lYDg. Left 5."1"'1:: ~-} )~}~ A(d~c~ 0\\ .si+e 6...1-06SS, ~nl\((' dtf'lA cr~fri; ?r~~e,n1 <h Co neGt ~Mpk~. D~p~ -h wt?tTer WGl..S "5.11 \ bn. £>~Y1 p1~ btAi1e~ <F..t07DtJ, Le.~ ~;t~ ~ 0703, TW4-24 08-29-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 l1 2 of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 ~ See instruction OENISONI)~~ WHITE MESA URANIUM MILL MINES FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I 3,-J\ ~~r+er GhlorCft~I'M .2.01.,2. Location (well name): L-1--r;_W_4_-_~~ ________ ----I Sampler Name and initials: 1 1'"~nnif 801LJ~~h1t Field Sample ID Date and Time for Purging I 47 t 0/20\ ~ and Sampling (if different) q/I// ~Dl~ L--~ __________ ----I Well Purging Equip Used: 11:1 Ipump or @] bailer Well Pump (if other than Bennet) I ...... Crr_""_I'l_a_to_' ~ ____ --' Purging Method Used: I 'il 12 casings @]3 casings Sampling Event IQUA.r+e..(·~ Gl1IDrl)f'~ryV} Prevo Well Sampled in Sampling Event L-1-r_VJ_'1_-_2.5 __ R __________ --' pH Buffer 7.0 7.0 pH Buffer 4.0 Y.O Specific Conductance 1-.1 _~.;..q_1,---__ ---,1 [!MHOS/ cm Well Depth(O.Olft): L..-ll_3'1_ • ...;;;.,g _b __ --' Depth to Water Before Purging 1 '"1~. 2.0 Casing Volume (V) 4" well:I SS' g~ 1(·653h) 3" Well: 0 (.367h) L--___ --' Conductance (avg) L-I ..;;.~...;~.....:.:::S::-1f--_____ --' pH of Water (avg) Well Water Temp. (avg) I }S .lio Redox Potential (Eh) 1-.1 _2=g-..:."_---' Turbidityl l;2. -77 Weather Condo Ext" Amb. Temp. O( (prior sampling event)L-1 _~_J_'_---' Time L-1'_.:2._] ~~_----I Gal. Purged Time L-~~_O __ --, Gal. Purged L-I/_DD __ ---' Conductance pH 1 """].J'1 Conductance 2.'1LJ pH I 1.18 Temp.oC 15>. q$ Temp.oC Js.y) Redox Potential Eh (mV) Redox Potential Eh (m V) 1 ...... :z:_'1_~ __ ---' Turbidity (NTU) I (; I I Turbidity (NTU) Time L-1l_2._.2J __ ---' Gal. Purged I ...... _UO ___ --' Time 1122.':>..... Gal. Purged l ...... l_2_0 __ ...... :t11 5 I pH 7 ./~ '---..,------' Conductance pH 1 . 1.20 Conductance Temp.oC 15·34 Temp.oC 1 )5.3$ Redox Potential Eh (mV) Redox Potential Eh (m V) 11-.~_g_3 __ ---, Turbidity (NTU) II.' Turbidity (NTU) I ) 1. 8 White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = L-I ~lD ___ ....J T=2V/Q= I I), \1 I Number of casing volumes evacuated (if other than two) 10 If well evacuated to dryness, number of gallons evacuated 10 Name of Certified Analytical Laboratory if Other Than Energy Labs L.I ,V,--=-'I;".;.A ______ ----I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs 1jJ 0 3x40 ml 0 ~ HCL ~ 0 Nutrients 111 0 100 ml 0 15 H2SO4 ~ 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) m 0 Sample volume 0 1tJ 0 El C\, \O('~~ C-If preservative is used, specify Type and Quantity of Preservative: Final Depth ..... 1 ".;;;.....;...~_. 1_'0 __ ----1 Sample Time ..... 1 O_b_5_O __ ----I Comment ~ See instruction 1.2.} O. () "42... T~i\Y\c,r t>..fl~ Cr6,.rr~f\ ?rc.s~iI-t +0 '011(';,+ SfA.Mpl(,~ . .D-e.pi-h 1-0 \tJtttlf w~ YCJ.ll. ObS,O, Le+1-Si+e. ~ ObSy TW4-25 09-10-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 ('---"'·--·------"··--'-'---'--···'·---·-1 I OENISONI)~~ I j MINES FIELD DATA WORKSHEET FOR GROUNDWATER ~ See instruction WHITE MESA URANIUM MILL Description of Sampling Event: 1 3("3\ QV\o-.(":h:(" G)., \O<tsro("J'V) !2.0\ ~ Location (well name): ",-I-r_w_~_-_~_S--,-R,,"-_______ ----I Sampler Name and initials: r::ro..nne"'-+l 0 n lilJl~/f~ Field Sample ID ITW~-.2.5R DQ'02012 Date and Time for Purging 1-1 '1..:.../_1_0-'-1_2.._0_1'2. _____ --' and Sampling (if different) N / A-"'----'-~------------~ Well Purging Equip Used: @Dpump or @] bailer Well Pump (if other than Bennet) 1 Z;~v..l1J\fo.s Purging Method Used: @]2 casings @]3 casings Sampling Event IQ v.o..l"+e<"\'-'\ G h \ or~o, M Prev. Well Sampled in Sampling Eventll-, __ W_4 __ -1_4 ___________ ---I pH Buffer 7.0 pH Buffer 4.0 4.0 Specific Conductance 1-1 4...;,.j..&..j-l--_____ ---'1 ~MHOS/ cm Well Depth(O.Olft): ..... 10 ____ ----1 Depth to Water Before Purging 1-1 _0 ___ ---' Casing Volume (V) 4" well:~_o ___ -fI (.653h) 3" Well:. D . (.367h) Conductance (avg) q.1 "'----'-----------' pH of Water (avg) Well Water Temp. (avg) 1 ~'-\.\D Redox Potential (Eh) ..... 1 ~_lf_~ __ -, TurbiditYI-I _0 ____ -' Weather Condo Ext'l Amb. Temp. O( (prior sampling event} ..... I ~_~_o __ ..... Time ..... 1 \_D_lf=-~_--, Gal. Purged 130 Time Gal. Purged Conductance 'i .1 pH 1 J.&l.( Conductance pH 1..-1 __ ----I Temp.oC 1 ~4.16 Temp.oC Redox Potential Eh (m V) "'--~....J51..1.1 __ ----, Redox Potential Eh (m V) ..... 1 ___ --' Turbidity (NTU) () Turbidity (NTU) I I Time Gal. Purged Time Gal. Purged Conductance pH Conductance pH ..... I ___ ...... Temp.oC Temp.oC Redox Potential Eh (mV) Redox Potential Eh (m V) .... 1 ___ --' Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged }50 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = &.....1 ---:..'0 ___ --' Time to evacuate two casing volumes (2V) T=2V/Q= 10 I Number of casing volumes evacuated (if other than two) 10 I If well evacuated to dryness, number of gallons evacuated 10 N arne of Certified Analytical Laboratory if Other Than Energy Labs I /V/A Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs ~ D 3x40 ml D ~ HCL 'IE D Nutrients l13 D 100 ml D ~ H2SO4 I!l D Heavy Metals D D 250ml D D HN03 D D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) ijJ D Sample volume D ID D 1lI 0h \D("~ ~e. If preservative is used, specify Type and Quantity of Preservative: Final Depth IL--..;;o ____ ...... Sample Time 10;2.0 Comment ~ See instruction A C'ri\'Je~ 0(\ ~;+e. a.. +-1000. -r()\()ner d'.n ~ &-o...r,ln ?("~.sen+ .for R;1')sfA+<' 1< J" ,S,G\1-( b~~d\r) ",i-1005. f\AI'V\'P.e.a 50 G-~JJ()f").S o.f' -Sl>"'f> wo..-t-~r ""F'\~ )00 G-t'A.l1<lTt.S' 6-P PI V-)",+er . 'R1t)~o..fc endea tA.t1~ 'sO\I'Vl?Je..s were. G~J)e.~+c:tA ~+ I02.~ .. L e~1-s iTt= ()..} 10;2.5. TW4-25R 09-10-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) ATTACHMENT 1-2 ~ See instruction j)ENISONI)~~ WHITE MESA URANIUM MILL MINI:S FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 13r l\ Qv..o.r=tcr Chlor;;J~rM .2612., Location (well name): L-11W __ '1_-_.2_, _________ ----I Sampler Name and initials: F"t;.nncr DD1JjJ~/I+f Field Sample ID Date and Time for Purging 1 q/lO)2..b1~ and Sampling (if different) 1t-...;.~.;;...J.....;I/.....;/.20_.:.....;I'<...~ ____ ___I Well Purging Equip Used: ~pump or @] bailer Well Pump (if other than Bennet) 1 &rl;\"J?6.s Purging Method Used: l'til 12 casings @]3 casings Sampling Event IQ\.Aa.r:ter6 G'hlorJ~( f"\ Prevo Well Sampled in Sampling Event I L-i1_W----.;y_-_2.5 ______ --I pH Buffer 7.0 110..-7..:..-.., b ___ ---I pH Buffer 4.0 1-1.0 Specific Conductance L-I ~tf'l...:..j-l--___ .....II !lMHOS/ cm Well Depth(O.Olft): 1 gb,ob Depth to Water Before Purging 1 r;, 3. 1..5 Casing Volume (V) 4" well:1 1 Li .Gl2, 1(·653h) 3" Well: 0 (.367h) L...-___ .....I Conductance (avg) b3S"D '--~~~-----------I pH of Water (avg) Well Water Temp. (avg) 1 )5. ~l 1 Redox Potential (Eh)1 qQ) lS.~l Turbidityla....;l...;..l C>~_----' Weather Condo IL---_'R_o..._r+--.;~=--_C_lo_wl___Y_t-----.....I Ext'l Amb. Temp. O( (prior sampling event)1 2.7° Time Gal. Purged )71.5D Time Gal. Purged Conductance 1 f>3 50 pH 1 Q,3D Conductance pH L-.1 __ -.....I Temp.oC I lS~~l Temp.oC Redox Potential Eh (m V) Il.-y_bS __ ---I Redox Potential Eh (m V) L-I ___ ----I Turbidity (NTU) I 1\0 Turbidity (NTU) Time L-I 0_7_0...;.7 __ ...... Gal. Purged Time 1.-10_7_'_'_----1 Gal. Purged .... 1 ___ ...... Conductance pH Conductance pH 1 4.4:J: Temp.oC 14. '10 Temp.oC 1 14 .'-13 Redox Potential Eh (mV) Redox Potential Eh (mV) I L-5_43 __ ----1 Turbidity (NTU) Turbidity (NTU) 1)6.\ White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Be.i~'e. V olume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I 10 T = 2V /Q = I .2, ef 4> I Number of casing volumes evacuated (if other than two) },1"1 If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs 1-1 ..;..,v....;/..Lfr~ _____ ---I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs ~ D 3x40 ml D ~ HCL ~ D Nutrients ~ D 100 ml D III H2SO4 1!J D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologies D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) f¥1 D Sample volume D IE D ~ 6hlor;~C If preservative is used, specify Type and Quantity of Preservative: Final Depth 1-1 ..l.j81,.;;:5;;.....;._{)~O __ ---I Sample Time D708 See instruction Comment TW4-26 09-10-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ~ See instruction Location (well name): 1...-1 11_W_'-1_-_2:_7 _________ --I Sampler Name and initials: 1==r;.f\Ylcr H6)hd~h1t Field Sample ID Date and Time for Purging 1 g7;2..472~J':l. and Sampling (if different) g/:30/:;.ol'A Well Purging Equip Used: OOpump or [QJ bailer Well Pump (if other than Bennet) 1 &f" \Af\ltfo..s Purging Method Used: rnJ2 casings [QJ3 casings Sampling Event I Q", .. rf.,.:S ch lor i*or 1Y\ Prev. Well Sampled in Sampling Event , Jy..J 1..J ~ :::t.. '1 pH Buffer 7.0 L-I _7_ .. _D ___ --I pH Buffer 4.0 YolO Specific Conductance 1...-1 _9_11---1..1 ___ ---'I~MHOS/ cm Well Depth(O.Olft): 1 4b.OD Depth to Water Before Purging 1 g2. '-\.5 Casing Volume (V) 4" well:1 g.~l1 1(.653h) 3" Well: 0 (.367h) '-----_ ...... Conductance (avg) ~4.3 pH of Water (avg) 7·DS Well Water Temp. (avg) I ) ~ • () 1 Redox Potential (Eh) 1 f2 '1 g Turbidity 1 Lf8.b Weather cond., I...-__ S_"'_~_n~ _________ ...... Ext'l Amb. Temp. O( (prior sampling event) ...... 1 _~_4_"D_----, Time 1 19~ Conductance 1 5.2. L:J..3 Temp.oC 1 ji.o I Gal. Purged ...... 1 _I _S __ ----' pH 1 7 ,65 Redox Potential Eh (m V) 1 ...... 2.---:...4A"'--_----' Turbidity (NTU) 1 Y& .(; Time 1 O/)~ Gal. Purged Conductance Temp.oC Redox Potential Eh (mV) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater Time Gal. Purged Conductance pH L-I __ ----' Temp.oC Redox Potential Eh (m V) 1...-1 ___ ---I Turbidity (NTU) Time I071:t 1 Gal. Purged Conductance E ;Z 7 ;r 1 pH ,--I _7...;....;;-'_0....1-1---1 Temp.oC J6 .. 3'l.1 Redox Potential Eh (m V) 1 "35:2 Turbidity (NTU) ( O. 2 1 f\ _, 1 of2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (OAP) 5etDCC Volume of Water Purged 7~ gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I ) D T = 2V/Q = I 1,7"-I Number of casing volumes evacuated (if other than two) 10.39 If well evacuated to dryness, number of gallons evacuated 1/:5 Name of Certified Analytical Laboratory if Other Than Energy Labs 1-1 ..L;J,.....;~...:...I\-...::...-_____ --' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs "S 0 3x40 ml 0 1J HCL 'KJ 0 Nutrients 'B 0 100 ml 0 "'EI H2SO4 ~ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) lJ 0 Sample volume 0 -E 0 "[J Gh10(;~G If preservative is used, specify Type and Quantity of Preservative: Final Depth 1L-....;.~_5_. O_ll __ ----I Sample Time .... 1 0_7_1=<. ___ --' Comment ~ See instruction A<"l\led. 0(\ srtc. 0..1-lL13D o:Ja.flner Ma G-~r("ln ff'e.sent -For f~rfJ-e.. f\)\("~e.. be~o.n "",1-JL:}33 l\ .. (~d wc)1 foy Y.5 ~cconA.s, PV.({,),a well d(~ ~ \,.)~1-Cf' J..)/AS cleM L~» SitG ~t 1~37. A1f\\lJ. 0(\ ~,\·h:. ~t oIOJ;,-r:.nl1~(a.nA 6-o.rdf) ?(,~C:I1+ -h GOnect Sa~?)es.. Dep+~ 10 ~~T~r\A)~ ~2..qO. ~I\M?\e~ k;lea o..t OilZ. Le:~-~;+< 6-.t 07)S TW4-27 08-29-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) r~·~-~. -~~~-~i)111 WHIT: !::s~~~~~~ MILL ~ See insmoction I MINES FIELD DATA WORKSHEET FOR GROUNDWATER Descrip;ion of Sampling Event: 1 3,(' J; Q\}Y~rf~ Gl1I0('of'Dr~ ~J~ Sampler Name Location (well name): 1 "'T\N4-"~ and initials: ::YQ..~hGr JJ()lllA~l--rJf Field Sample ID 1'Tv-) y -60_ 09 132.012. Date and Time for Purging 1 &\/13/2.0 } '2-and Sampling (if different) Well Purging Equip Used: @]pump or @] bailer Well Pump (if other than Bennet) 1 ~/4 Purging Method Used: @]2 casings @]3 casings Sampling Event I Q"'r..r +« 1 "\ C:~) or btorM I Prev. Well Sampled in Sampling Event I -r IN L.\-62. pH Buffer 7.0 Specific Conductance 1 ........... 1 ..... 1 q"'--___ --'I !lMHOS/ cm Depth to Water Before Purging L-I _() ___ --' Conductance (avg) 0./ L--_~~ _____ --' pH Buffer 4.0 1 g.D Well Depth(O.Olft): .... 1 _D ___ ----' Casing Volume (V) pH of Water (avg) 4" well:~_?J-----1I (.653h) 3" Well:. 0 . (.367h) Well Water Temp. (avg) 1 z.~:~S Redox Potential (Eh) .... 1 ~_3_~ __ --, Turbidity ..... l_l _,O __ ---' Weather cond.; L-_C_' _c_oJ _________ --' Ext'l Amb. Temp. O( (prior sampling event}I .... a._l 0 __ .....1 Time 1 0 ~.sl..\ Gal. Purged Time Gal. Purged Conductance O. 7 pH '71 b((; Conductance pH L..-I __ --' Temp.oC Temp.oC Redox Potential Eh (m V) 1::33 Redox Potential Eh (mV) .... 1 ___ ----' Turbidity (NTU) Turbidity (NTU) Time Gal. Purged Time Gal. Purged Conductance pH Conductance pH .... I ___ ...... Temp.oC Temp.oC Redox Potential Eh (m V) Redox Potential Eh (mV) 1 .... ___ ----' Turbidity (NTU) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged o gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I 0 T=2V/Q= 1 0 I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated o N arne of Certified Analytical Laboratory if Other Than Energy Labs IL--.,v)_m _______ ---I Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y VOCs )!] 0 3x40 ml 0 ~ HCL ~ Nutrients t1 0 100 ml 0 llJ H2SO4 tI Heavy Metals 0 0 250 ml 0 0 HN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) 1tI 0 Sample volume 0 lJ 0 0hlof;1~ If preservative is used, specify Type and Quantity of Preservative: Final Depth 1-1 __ 0 ___ ---' Sample Time Comment ~ See instruction .tIff;"C! ;" \"~.J og~,t -kn~~r ltoll;j~ fre~ellf -to L611ecl-.s"'YY\f JeS" -rOOK \ S6-of' f'~r"""".Jcrs ~J., ~cVY/'plc5, coIJec.}d-.J-(;~:5S L~-} LtAb Ov~ oq()O TW4-60 09-13-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) r--------·---l ATTACHMENT 1-2 J'j)ENISONI)~~1 WHITE MESA URANIUM MILL ~ See instruction 1 MINES FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I :3 ... J;; QtJ~~+e.r 6\....' or6{'df"yV\ -eO} 1. Location (well name): I C'\ W....l :s 2 (ru.JI-/-tr) Sampler Name and initials: Field Sample ID Date and Time for Purging I 09105/ 1,0) ~ and Sampling (if different) NA Well Purging Equip Used: ~pump or [gJ bailer Well Pump (if other than Bennet) Purging Method Used: [gJ2 casings [gJ3 casings Sampling Event I ~ v .. ~h,,. \)' [, '" lor 61' II elM Prev. Well Sampled in Sampling Event I T v.> I..> I ~ 0 t..J pH Buffer 7.0 7,,0 Specific Conductance I q q q I~MHOS/cm Depth to Water Before Purging I 74« y 5 I Conductance (avg) pH Buffer 4.0 Well Depth(O.Olft): Casing Volume (V) pH of Water (avg) 4" well:1 :3 6~6. 3" Well:. 0 IC.653h) (.367h) Well Water Temp. (avg) Redox Potential (Eh)1 1 6 L] Turbidity I 7, J Weather cond·1 L-__ S __ U_v'\_vv-----:'1:....--_____ ----I Time IY3.5 Gal. Purged I --; 2J& q I Conductance p ~:SJ pH I 6.,t2. I Temp.oC )$ .. 7£ I Redox Potential Eh (m V) 161 Turbidity (NTU) Time I , t:J 3 7 I Gal. Purged Conductance :J K 2~ pH Temp.oC Redox Potential Eh (mV) Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater I 73.,J:2 &,,£7 Ext'l Amb. Temp. O( (prior sampling event)1 20 D Time I t Y :3 I; I Gal. Purged I 72. .. Q 11 Conductance l ::z tJ. {I pH I 6.1£R I Temp.oC 15: t7J I Redox Potential Eh (m V) I 16 Y Turbidity (NTU) Time I \1:/ :3 x> Gal. Purged Conductance l :::b ? ~7 I pH I Temp. °c I L5. q UJ I Redox Potential Eh (mV) I 167 Turbidity (NTU) ---; " 2 ,:?,34i 6"S.7 I 1 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged 73.7~ gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S160= I ~ :217 T=2V/Q= I :337" tt3 I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated N arne of Certified Analytical Laboratory if Other Than Energy Labs 1...---:::..#.::....424:...1.-____ ---1 Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) Y N Y N VOCs I5It' 0 3x40 ml 0 ~ HCL ~ 0 Nutrients ~ 0 100 ml 0 ~ H2SO4 12! 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250 ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) OJ 0 Sample volume 0 5f 0 ~ ~k~Dr; ~G If preservative is used, specify Type and Quantity of Preservative: Final Depth I 7 Cf tI q 3> Sample Time Comment ~ See instruction TW4-65 09-05-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 r·······_········ ·································_···············_·-1 !()ENISONI)~~1 L.~INES FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 13 rCK Q"'CArfer G"hloro+6f"rYl 2..0)2.. ~ See instruction WHITE MESA URANIUM MILL Location (well name): L-1-T"_W_t1..:,....-_7....;.O _________ ---' Sampler Name and initials: I ~nr'ler Rl51IJa~.I11t Field Sample ill I-nNY-70 ... 0Cf11~OI:l. Date and Time for Purging I <'17\O/~D12 and Sampling (if different) Well Purging Equip Used: OOpump or [QJ bailer Well Pump (if other than Bennet) I Vr-lAi\Jfo.s Purging Method Used: 002 casings [QJ3 casings Sampling Event I (51", .. r1-e.rl,:3 L.l-< \ orof'or>Y\ Prevo Well Sampled in Sampling Event I.., W Lj ~ 2S R pH Buffer 7.0 7,"0 pH Buffer 4.0 Y.O Specific Conductance lL--q_~_q ____ .... 1 !!MHOS/ cm Well Depth(O.Olft): I \ 3L4. gO Depth to Water Before Purging I Lj 9. Q...b Casing Volume (V) 4" well:i p5. g'f i(·653h) 3" Well: () (.367h) L--___ ---I Conductance (avg) 2-q £.7 L--~~~ _____ ~ pH of Water (avg) 7 .1q L--_~ _____ ~ Well Water Temp. (avg) I \5, '1 D Redox Potential (Eh)1 ~8~ Turbidity I \~, 77 Weather Condo Ext'l Amb. Temp. O( (prior sampling event}L-1 _1:..:..;..7_o_----J Time Gal. Purged Time I I Gal. Purged I I Conductance pH Conductance I I pH I I Temp.oC Temp.oC I I Redox Potential Eh (mV) Redox Potential Eh (mV) I I Turbidity (NTU) Turbidity (NTU) I I Time Gal. Purged Time I I Gal. Purged I I Conductance pH Conductance I I pH I I Temp.oC Temp.oC I I Redox Potential Eh (mV) Redox Potential Eh (mV) I I Turbidity (NTU) Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 6/06/2012 Rev. 7.2 Groundwater Monitoring Quality Assurance Plan (QAP) V olume of Water Purged t2.0 gallon(s} Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I 10 T = 2V/Q = I n. )"1 I Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated o N arne of Certified Analytical Laboratory if Other Than Energy Labs # / It ~----------------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N Y N VOCs TfJ D 3x40 ml D elf HCL ~ D Nutrients It) D 100 ml D I1i H2SO4 00 D Heavy Metals D D 250ml D D HN03 D D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) rn D Sample volume D ~ D ~ ~h 'D,~aL If preservative is used, specify Type and Quantity of Preservative: Final Depth I bl:, I l D Sample Time Comment ~ See instruction TW4-70 09-10-2012 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 TabC Weekly and Monthly Depth to Water Data Date 7/2/:;LO 12- Time Well \'3t.i3 MW-4 i'=S:sq MW-26 '336 TW4-19 1335 TW4-20 13117 TW4-4 Water: Depth to Water Name ~"ner »6Il'~i Depth Comments 7[),~O Flow L-}. Lf G-PM Meter K 757' 5<4 .. ()S Sg,4u Flow 10.g G-?M Meter 23~LJ ,\17 bO ,l3 Flow ) Y.O G-P 1'-\ Meter " l-r7S73~ .03 Sb _b;iS Flow 16.S0 &PM Meter yq \3:2.1 . 'l r; b~lg~ Flow 93 C-PM Meter K.2Xl }9 .S0 .':::>-0 0 b.e Y Depth to Water Date 7 J q / I ;), , I Time Well Depth Comments \1)...07 MW-4 7'.70 Flow 1.4.3 C.PM Meter «52.' V\. <{5 , ,,"-o'-{ MW-26 81.:2.0 Flow 10.J.. <;~J1 Meter 2.~'i(,&q:1' t"'lDI TW4-19 go.so Flow 14.0 6--P~ Meter Y YIt" ,3.00 11..00 TW4-20 5& .so Flow \O.l &1M Meter 4Q309'-1 A 7t:t I '.' TW4-4 G,Cf.ttS Flow g·3 ~\ 1°1/\ "'1'" Meter 1S3"f3~ l.!)l) Water: :2 \\31.1 ~ Date J II f! I ;L Time Well 131S MW-4 i3i i MW-26 1362 TW4-19 1361 TW4-20 1 ~I ~ TW4-4 Water: '] \\OO~IJ- r Depth to Water Depth Comments /2 -A' ('") Flow L--f. LJ r;-O;V\ Meter <if: !fq '6 7S ... 3D 98, L.--I.~ Flow 11. ... 5 /-rf .k1 Meter J/) .-;> .L.. ~~A! );' y! ;-z::" >" (::;- 67~ i? Flow 14.6 kf'A Meter .502-6;;7.06 l)cf. D D Flow 10,2 I~fj./l Meter '--I q '-II q q _ "3 0 I 6q.lO Flow 10.0 G-P)A Meter .2 ~I 0..5 Cf.2 ~ OL1 ;).2 \ :rti () Depth to Water Date 7/:23 / I J.- Time Well Depth Comments 1:1:?J 7 MW-4 '-7\.YO Flow LL3 ~pM Meter 39'Lf 7q~ £5 L~3L?) MW-26 h1.70 Flow [0-6 C-PM Meter ;1.38£0/.O"t 11115 TW4-19 65 ,/5 Flow )4.0 (SPM Meter 51bD)6,07 1:22.'1 TW4-20 SG ,q \ Flow i6.L\ C-P J-ll Meter 1Cf£3G7,b5 I i'1 Y \ TW4-4 £'i.qq Flow ?5 .C( Cpf-l't Meter 8Y~67q ,56 Water: 22K&b1 Depth to Water Time Well Depth Comments )':)iY MW-4 71.:20 Flow Ll .3 GPM Meter qO)575/f:Z 12->\0 MW-26 5q.~O Flow 10 .3irPM Meter 2.yoL{(Y3.~~ )'-150 TW4-19 ~() 51 Flow I f.(~ () frP}l1 Meter S;tgS77.0i 13 0 ,=-TW4-20 S6.3,0 Flow 16 .~ (rPM Meter yq30b~' 15 :~ l6 TW4-4 bq,qS Flow g .. q 6-P){ Meter gS2.17b.!{O Water: 1 3;2.'101 .,./ j /5' ... ./Li I'": I (7 Chloroform Wells Date 7(rl J jt)- Time Well De~th Comments IJ.:2l MW-4 7;1.,Di 1 '-;2~ TW4-1 ()' L-) .' it 1.320 TW4-2 ~ 2 '\ 6 (, ~CJ 1210. TW4-3 ,,=S O.()D 11,?-~ TW4-4 /q 3'Q I; '. ;313 TW4-5 .56" S~ I.Y :1 1 TW4-6 6C:i ~ f?~' 13 22. TW4-7 6 7 . ()c( IJ;)"~ TW4-8 ,;{6.Sr> 1311 TW4-9 -; y ~ L-/ K J J.l-';-TW4-10 st;. 8 3 11.ID TW4-11 <;£, I I 13 3 5-TW4-12 yo .QO 1_)-) / TW4-13 Y l <jQ 1.3~3> j TW4-14 S6 .,t;R ISl3 TW4-15 76.05 1~C>i "1 _.$ C5T 6::i. TW4-16 ·5 C[.50 1 ]CY~7 TW4-17 -"Jy s'-/ .... ~ l;LS;;?. TW4-18 57.05 1.Jl.-i 0 TW4-19 6Cj , ~J t1 13Yt-J TW4-20 56".76' i:.Lt;,5 TW4-21 ~~Y., 1,5 l3D~ TW4-22 5~3. 2.2. If;v6. TW4-23 iL{ ~~) L; .~ v l:3o:2 TW4-24 ~Lf ~/~ 4~"C J 2.1; 8:' TW4-2S ~u? ~5 i ~3' ~3a TW4-26 /' or o3c.2:> I 3i-1 I IvV L-{ -;L/ d/) Dc7'~6 ( - Depth to Water Time Well Depth , Comments / () :;J.,,~ MW-4 7h<i:lt-f Flow Y .. 3 &P/-'\. Meter qJ2YO~.i7 10 'I_Cj I rr--MW-26 ~r;8 ~ 6 __ 0 Flow IOe IS &Pr\ Meter 2Y215KL27 1 () ,t:;'y TW4-19 ~~!'f g':2. Flow I~-. '" / L{ "D b-f/V\. ~-~ ./, ,..!. Meter ;:; ""....,--..... -...... ~ :;; -= ' -" --" ""-.)r.t :z.~~ q 1. ' j D ,?--.'S TW4-20 b6~l7 Flow l() .. :L (~f,;V\ Meter 50(-:> 211..'_ 6 A losb TW4-4 75.8q Flow ~.4 " ptJ &.// Meter bOS6S#S ,. Water: ~-s6 '7i I Depth to Water Time Well Depth Comments i~-;I MW-4 7/9i1L.1 Flow y.1.-1 frrDA Meter QJ<g.::;'[7 .. 23 1)17 MW-26 t5elO Flow j ,2" 1 bP~ Meter ,21-1'-1 t; 62" 7~ l~l~ TW4-19 ~'l .. 74 Flow 111 (;..P y\ Meter £56:2.0[5 .. 00 l :::t~~ TW4-20 ~7 .b( Flow 10 ,,5 GP)./\ Meter S;0179 '7.0 Y 12'56 TW4-4 hq,86 Flow ''''~o (;PA Meter gb615i~q/ Water: 2Y}}CfR epth to Water ,., Date 8' I ~o /1 ,Y- Time Well Depth Comments \"1li MW-4 I), .2.5' Flow L{i3 Meter ~u.y 'C(2. LfS gO,2-£ \, 1 '~}1) MW-26 S<1.b5 Flow 10,i..\ G PiV\ Meter ~ L\ (, [ Y7 . .25 I J Lj L--1 TW4-19 6'C)~Df? Flow' 1l,./.D brA Meter _L;6i '76 I _ 0 0 130'S TW4-20 .5 (,. b5 Flow 10d.. G-Ptvi Meter SO~ I '-ib,S~ I r~~;;2.0 TW4-4 (4,q~ Flow )O,S 6-P}:.\ Meter 671LJ7 0,70 Water: 26 ""3.55'0 Time Well l3!:>1-( MW-4 '35r; TW4-1 I~S~ TW4-2 , 13i-.l1 TW4-3 }r~~ \391 TW 4-4 13Y3 TW4-5 lib1 TW4-6 13.5) TW4-7 J3YQ TW4-8 13L.J}; TW4-9 r\YJ TW4-10 i3SJ TW4-11 iYOL1 TW4-12 1406 TW4-13 IYb f TW4-14 !S~D TW4-15 J ~1'33 TW4-16 jL.-135 TW4-17 11-/27 TW4-18 I t-j i-16 TW 4-1 9 133 f) TW4-20 !t.i3b TW4-21 1326 TW4-22 tLi 1 ~ TW4-23 i~13l.--1 TW4-24 iY1Lj TW4-25 \1.\\.6-TW4-26 ~~ :J~fO _ Iwt-f-27 Chloroform Wells Depth gO ,35 b9 .QQ 56 .53 b'L71 f¥g~07 fb.Y/ 5S,75 rY6 g7_5 qg<5Q w59 .. 2Q (Y. Yo ;;-7,,0/ AD.Ot ..56-73 S',-\. ;;.7 53 ~D2 bL\,t.\~ Comments Depth to Water Time Well Depth Comments J L-[ 0 I MW-4 7~·. IrS Flow L}~ :3 Gf/V\ Meter q.3QQQ3 .l6 1?I-fY MW-26 t;,>5. '7;: Flow 1(" / I L/? (;-p)/\ Meter 2SD3 '3f?-c (? I ()_0U TW4-19 ~5C:L 7'1 Flow ' 14 .. 0 6-Py\. Meter SC,7:2.61 ~ DO 133c) TW4-20 .~'6 . ~)5 Flow {("") if h (~P7'\ Meter ~{J6')(7 2 c;!6 ( I 1..-11.>' TW4-4 .tg f tL tiL> Flow C? L-{ 06 l GP /p't Meter <lgu6 ~ Ct /'--' /-. I. U Water: '3 i ;;l 5. S ;3 Depth to Water Date 9 -10 -I ?-.. Time Well Depth Comments 0 r?'::;-j MW-4 72.l15' Flow L{ 11 6-P/"\. Meter C; 4si l _~. ? 9 6 g y g MW-26 h't; -i5 Flow 252oer~. 7{) Meter 10.1 6--y.~./"'\ TW4-19 Flow ' ~ } '-I .e G fj./\ , ... Meter () ~ L.16 TW4-20 .5 q.3 ~ Flow le.::> {; Pj'\.A.. Meter _{D f;Z 3D ~'f {)Q'.5 3 TW4-4 r5"q, ((7 Flow K-2. 6 f/Vt Meter fX' q Lf() I ,~() Water: ''"7 .-:?""" L{ ('" ~ .,) '..::> _~ ."~ L) Depth to Water Date q /17 / J .2 Time Well Depth Comments ) 1-1 L-{ /; MW-4 72.DY Flow Y.L\ 6·P/v\ Meter Cr .5 :> I gS. Y L-f '/ L.J /...1.3 MW-26 .. S 7 .. /; q Flow I L:L ;.;f fA Meter QS'3rt.-12 :s o l ,~('''~ E 3 .y f ~t9-TW4-19 _-/~4-t-I-.-b--~.. -, 'I Flow ~"" ... 6ef5.~~ iY .O &f/-1. Meter -t'? ~ ... 62 ~ ~ , "I:: ' ",' ---r-.$=-""" . '2f.., ./ "UZ-'-"WCI ,-0 'jC':::' .. C't') I L../ /...f I TW4-20 6D ~Ll o Flow 1 6-~ (; I>,-fo1 Meter SiOO77.7i i W,,-,7. 6q~ 4 1 X' -~ TW4-4 ~:> Flow ~ -,. {f.g &P~ I I: T~,.,.yo---4' ..... ..... I Meter ~ Qq bb {,q. i..{( Water: .3i..Ib. 77 D Depth to Water Time Well Depth Comments 1:;2)..0 MW-4 11. tt'l Flow L-\u c? t~p,/-/l Meter q 6 ;;Z l '37 ,6' g f2-l r MW-26 ~'\ .tt5 Flow 1 [J, 7 G-P.AA Meter 2,56 y 7~'L i 7 ~ \ 2.l-\S TW4-19 b3.41 Flow ' )1;.0 lrPM Meter ~3732..8.C.b bD.~~ r;2../6 TW4-20 ~7 Flow 10 . ..5 6-P/~ Meter ~5 j). f t?-q~~~ q I I 12J-Y TW4-4 ;;"q, LJ I Flow r;?.b fyl?Jv\. Meter q c' ;,. 7 7f;, It I Water: ~S6371-4 Depth to Water Date 10/' /~() 12.. Time Well Depth Comments I~"'''' MW-4 ~O.:26 Flow '1·3 6.-PI-'\ Meter q'7:]qO.cq'J I MW-26 5S.;D Flow (6.5 ra~ Meter .2bi"'1 ~,. ''3 pet r.\0, TW4-19 51. is Flow Ilf.O c..PI'\ Meter b-''''7071.00 1~~5 TW4-20 Sc...30 Flow ID.~ CfiH Meter ,&1)3'-16.52 13lf~ TW4-4 7~'iq Flow R.Y. 6-PM Meter q()~J~5.8a Water: 33J~qQ TabD Kriged Current Quarter Groundwater Contour Map, Details Map, and Depth to Water Summary TIME WELL 832 MW-1 1127 MW-2 1324 MW-3 1325 MW-3A 1032 MW-5 1027 MW-11 1036 MW-12 1009 MW-14 1011 MW-15 1331 MW-17 829 MW-18 759 MW-19 1308 MW-20 1300 MW-22 1043 MW-23 1124 MW-24 1005 MW-25 1103 MW-26 841 MW-27 1121 MW-28 1046 MW-29 1049 MW-30 1059 MW-31 1053 MW-32 1018 MW-33 1014 MW-34 1041 MW-35 1015 MW-36 1012 MW-37 Static level 64.30 109.80 83.11 85.15 106.45 87.85 108.49 103.71 106.45 74.36 70.17 54.19 85.63 67.05 114.15 114.25 73.55 74.59 51.46 76.45 101.95 75.82 67.81 74.36 dry 107.94 112.35 110.46 107.25 NAME: Tanner Holliday, Garrin Palmer DATE: 9/27/2012 TIME WELL 944 MW-4 942 TW4-1 945 TW4-2 938 TW4-3 949 TW4-4 935 TW4-5 948 TW4-6 943 TW4-7 940 TW4-8 937 TW4-9 932 TW4-10 947 TW4-11 952 TW4-12 954 TW4-13 956 TW4-14 1103 TW4-15 1101 TW4-16 1053 TW4-17 849 TW4-18 730 TW4-19 932 TW4-20 857 TW4-21 931 TW4-22 1055 TW4-23 929 TW4-24 845 TW4-25 1057 TW4-26 958 TW4-27 Static Level 72.04 64.85 67.26 50.15 70.13 56.81 69.74 68.17 66.55 54.67 55.95 56.96 41.09 46.90 86.45 74.59 59.37 74.36 57.30 59.99 59.95 54.19 53.10 64.45 54.70 49.31 63.11 82.35 TIME 801 756 752 1004 1001 847 842 746 750 834 824 837 826 804 822 818 815 807 810 821 814 811 743 1154 WELL PIEZ-1 PIEZ-2 PIEZ-3 PIEZ-4 PIEZ-5 TWN-1 TWN-2 TWN-3 TWN-4 TWN-5 TWN-6 TWN-7 TWN-8 TWN-9 TWN-10 TWN-11 TWN-12 TWN-13 TWN-14 TWN-15 TWN-16 TWN-17 TWN-18 TWN-19 Static Level 62.08 27.04 41.47 47.74 42.75 53.06 23.66 34.00 43.40 69.55 75.17 87.86 62.20 62.60 80.85 69.50 27.34 45.81 62.46 91.91 47.71 33.79 57.95 52.50 TIME WELL Static Level NA DR-1 ABANDON NA DR-2 ABANDON 1203 DR-5 83.11 1207 DR-6 94.44 1021 DR-7 92.22 1216 DR-8 51.05 1212 DR-9 86.52 1210 DR-10 78.1 1317 DR-l1 98.3 1321 DR-12 88.85 1328 DR-13 69.99 1227 DR-14 76.39 1312 DR-15 93 NA DR-16 ABANDON 1230 DR-17 64.97 NA DR-18 ABANDON 1234 DR-19 63.25 1245 DR-20 55.5 1251 DR-21 107.37 1238 DR-22 Dry 1248 DR-23 70.66 1241 DR-24 43.84 NA DR-25 ABANDON @ estimated dry area M.W-S perched monitoring well showing 5503 elevation in feet amsl TW4-12 temporary perched monitoring well 0 5583 showing elevation in feet amsl TWN-10 ~5586 temporary perched nitrate monitoring well showing elevation in feet amsl PIEZ-1 perched piezometer showing ~ 5593 elevation in feet amsl TW4-27 temporary perched monitoring well ~ 5526 installed October, 2011 showing elevation in feet amsl RUIN SPRING 0 5380 seep or spring showing elevation in feet amsl HYDRO GEO CHEM, INC. NOTE: MW-4, MW-26, TW4-4, TW4-19, and TW4-20are pumping wells KRIGED 3rd QUARTER, 2012 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H :/718000/nov121UwI0912.srf D-l ",,',,:.,,;,,' " "",, " I I I I I I I I estimated capture zone boundary stream tubes resulting from pumping ® estimated dry area M.W-S perched monitoring well showing 5503 elevation in feet amsl TW4-12 temporary perched monitoring well 0 5583 showing elevation in feet amsl TWN-10 A 5586 temporary perched nitrate monitoring V well showing elevation in feet amsl PIEZ-1 perched piezometer showing ~ 5593 elevation in feet amsl TW4-27 temporary perched monitoring well ~ 5526 installed October, 2011 showing elevation in feet amsl RUIN SPRING b 5380 seep or spring showing elevation in feet amsl HYDRO GEO CHEM, INC. NOTE: MW-4, MW-26, TW4-4, TW4-19, and TW4-20 are pumping wells KRIGED 3rd QUARTER, 2012 WATER LEVELS AND ESTIMATED CAPTURE ZONES WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H:/718000/nov121UwI0912cz2.srf 0-2 EXPLANATION ,.,. ,.,. ,',' ,',' , , " I I I I I I I , estimated capture zone boundary stream tubes resulting from pumping MW-4 h d .. h' • 5550 perc ~ ~onltonng well sowing elevation In feet amsl T~-~554 temporary perched monitoring well showing elevation in feet amsl PI EZ-2 perched piezometer showing ... 5602 elevation in feet amsl TW4-27 temporary perched monitoring well ~ 5526 installed October, 2011 showing elevation in feet amsl HYDRO GEO CHEM, INC. NOTE: MW-4, MW-26, TW4-4, TW4-19 and TW4-20 are pumping wells APPROVED KRIGED 3rd QUARTER, 2012 WATER LEVELS AND ESTIMATED CAPTURE ZONES WHITE MESA SITE detail rna DATE FIGURE H :/718000/nov12/UwI0912cz.srf 0-3 TabE Kriged Previous Quarter Groundwater Contour Map @ Estimated dry area M.W-S perched monitoring well showing 5503 elevation in feet amsl TW4-12 temporary perched monitoring well 0 5577 showing elevation in feet amsl TWN-10 <)5586 temporary perched nitrate monitoring well showing elevation in feet amsl PIEZ-1 perched piezometer showing ~ 5594 elevation in feet amsl TW4-27 temporary perched monitoring well ~ 5525 installed October, 2011 showing elevation in feet amsl RUIN SPRING b 5380 seep or spring showing elevation in feet amsl HYDRO GEO CHEM, INC. NOTE: MW-4, MW-26, TW4-4, TW4-19, and TW4-20 are pumping wells KRIGED 2nd QUARTER, 2012 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE H:/718000Iaug121UwI0612_rev,srf FIGURE E-l TabF Hydrographs of Groundwater Elevations Over Time for Chloroform Monitoring Wells ....... tv o ....... o o Depth Below Measuring Point (ft.) 00 o 0"1 o ~ o tv o 0 09/25/79 02/06/81 06/21/82 11103183 03/17/85 07/30/86 12/12/87 04/25/89 ~ 09/07/90 ~ ~ 01/20/92 ~ 06/03/93 ....... ~ ""'l 10/16194 0 ~ "'C 02/28/96 ....... =-0 07/12197 < ~ ""'l 11124/98 ~ ... 9 04/07/00 ~ ~ 08/20101 ~ 0--01102103 9 "'C '-' 05/16/04 09/28/05 02/10107 06/24/08 11/06/09 03/21/11 08/02/12 12/15/13 04/29/15 00 V'I 00 o Depth Below Measuring Point (ft.) -......l V'I -......l o 0\ V'I 0\ o V'I V'I V'I 0 11108/99 04/06/00 09103/00 01131101 06/30101 11127/01 04/26/02 09/23/02 02/20103 07/20103 ~ 12/17/03 ~ ,&;0. 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S :c I!::! --~ S ~ ;... ~ ~ 0 ..:: .... c.. ~ ~ ;... ~ .... ~ t-N I ~ ~ ~ lIl8 I10I lIl6l/80 liiOIlLO lIlIl60 lIlIO/PO lIlI I1ZO I I1£l/lI I I1£O/I I 1 , o c: M 00 "-~ ~ ~ ~ o o -q: 00 o o tri 00 o o ..0 00 o o r-...: 00 ~ ~ ~ o o 00 00 o o 0\ 00 o o 6 0'\ TabG Depths to Groundwater and Elevations Over Time for Chloroform Monitoring Wells Water Levels and Data over Time White Mesa Mill -Well MW 4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,620.77 5,622.33 1.56 123.6 5,527.63 09/25/79 94.70 93.14 5,527.63 10110/79 94.70 93.14 5,528.43 01110/80 93.90 92.34 5,529.93 03/20/80 92.40 90.84 5,528.03 06117/80 94.30 92.74 5,528.03 09115/80 94.30 92.74 5,527.93 10/08/80 94.40 92.84 5,527.93 02112/81 94.40 92.84 5,525.93 09/01/84 96.40 94.84 5,528.33 12/01/84 94.00 92.44 5,528.13 02/01/85 94.20 92.64 5,528.33 06/01/85 94.00 92.44 5,528.93 09/01/85 93.40 91.84 5,528.93 10/01/85 93.40 91.84 5,528.93 11/01/85 93.40 91.84 5,528.83 12/01/85 93.50 91.94 5,512.33 03/01/86 110.00 108.44 5,528.91 06119/86 93.42 91.86 5,528.83 09/01/86 93.50 91.94 5,529.16 12/01/86 93.17 91.61 5,526.66 02/20/87 95.67 94.11 5,529.16 04/28/87 93.17 91.61 5,529.08 08114/87 93.25 91.69 5,529.00 11120/87 93.33 91.77 5,528.75 01126/88 93.58 92.02 5,528.91 06/01/88 93.42 91.86 5,528.25 08/23/88 94.08 92.52 5,529.00 11102/88 93.33 91.77 5,528.33 03/09/89 94.00 92.44 5,529.10 06/21/89 93.23 91.67 5,529.06 09/01189 93.27 91.71 5,529.21 11115/89 93.12 91.56 5,529.22 02/16/90 93.11 91.55 5,529.43 05/08/90 92.90 91.34 5,529.40 08/07/90 92.93 91.37 5,529.53 11113/90 92.80 91.24 5,529.86 02/27/91 92.47 90.91 5,529.91 OS/21/91 92.42 90.86 5,529.77 08/27/91 92.56 91.00 5,529.79 12/03/91 92.54 90.98 5,530.13 03117/92 92.20 90.64 5,529.85 06111192 92.48 90.92 5,529.90 09113/92 92.43 90.87 Water Levels and Data over Time White Mesa Mill-Well MW4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,620.77 5,622.33 1.56 123.6 5,529.92 12/09/92 92.41 90.85 5,530.25 03/24/93 92.08 90.52 5,530.20 06108/93 92.13 90.57 5,530.19 09/22/93 92.14 90.58 5,529.75 12114/93 92.58 91.02 5,530.98 03/24/94 91.35 89.79 5,531.35 06115/94 90.98 89.42 5,531.62 08118/94 90.71 89.15 5,532.58 12/13/94 89.75 88.19 5,533.42 03116/95 88.91 87.35 5,534.70 06/27/95 87.63 86.07 5,535.44 09/20/95 86.89 85.33 5,537.16 12111195 85.17 83.61 5,538.37 03/28/96 83.96 82.40 5,539.10 06107/96 83.23 81.67 5,539.13 09/16/96 83.20 81.64 5,542.29 03/20/97 80.04 78.48 5,551.58 04/07/99 70.75 69.19 5,552.08 05111199 70.25 68.69 5,552.83 07/06/99 69.50 67.94 5,553.47 09/28/99 68.86 67.30 5,554.63 01103/00 67.70 66.14 5,555.13 04/04/00 67.20 65.64 5,555.73 05/02/00 66.60 65.04 5,556.03 05111100 66.30 64.74 5,555.73 05115/00 66.60 65.04 5,555.98 05/25/00 66.35 64.79 5,556.05 06109/00 66.28 64.72 5,556.18 06/16100 66.15 64.59 5,556.05 06/26100 66.28 64.72 5,556.15 07/06100 66.18 64.62 5,556.18 07113/00 66.15 64.59 5,556.17 07118/00 66.16 64.60 5,556.26 07/25/00 66.07 64.51 5,556.35 08/02/00 65.98 64.42 5,556.38 08/09/00 65.95 64.39 5,556.39 08115/00 65.94 64.38 5,556.57 08/31100 65.76 64.20 5,556.68 09/08/00 65.65 64.09 5,556.73 09113/00 65.60 64.04 5,556.82 09/20100 65.51 63.95 5,556.84 09/29/00 65.49 63.93 5,556.81 10105/00 65.52 63.96 Water Levels and Data over Time White Mesa Mill-Well MW4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,620.77 5,622.33 1.56 123.6 5,556.89 10112/00 65.44 63.88 5,556.98 10119/00 65.35 63.79 5,557.01 10/23/00 65.32 63.76 5,557.14 11109/00 65.19 63.63 5,557.17 11114/00 65.16 63.60 5,556.95 11121/00 65.38 63.82 5,557.08 11130/00 65.25 63.69 5,557.55 12/07/00 64.78 63.22 5,557.66 01114/01 64.67 63.11 5,557.78 02/09/01 64.55 62.99 5,558.28 03/29/01 64.05 62.49 5,558.23 04/30101 64.10 62.54 5,558.31 05/31101 64.02 62.46 5,558.49 06/22/01 63.84 62.28 5,558.66 07/10101 63.67 62.11 5,559.01 08/20101 63.32 61.76 5,559.24 09119/01 63.09 61.53 5,559.26 10102/01 63.07 61.51 5,559.27 11108/01 63.06 61.50 5,559.77 12/03/01 62.56 61.00 5,559.78 01/03/02 62.55 60.99 5,559.96 02/06102 62.37 60.81 5,560.16 03/26102 62.17 60.61 5,560.28 04/09/02 62.05 60.49 5,560.76 05/23/02 61.57 60.01 5,560.58 06/05/02 61.75 60.19 5,560.43 07/08/02 61.90 60.34 5,560.44 08/23/02 61.89 60.33 5,560.71 09111/02 61.62 60.06 5,560.89 10/23/02 61.44 59.88 5,557.86 11122/02 64.47 62.91 5,561.10 12/03/02 61.23 59.67 5,561.39 01109/03 60.94 59.38 5,561.41 02/12/03 60.92 59.36 5,561.93 03/26103 60.40 58.84 5,561.85 04/02/03 60.48 58.92 5,536.62 05/01/03 85.71 84.15 5,528.56 06/09/03 93.77 92.21 5,535.28 07/07/03 87.05 85.49 5,534.44 08/04/03 87.89 86.33 5,537.10 09111/03 85.23 83.67 5,539.96 10102/03 82.37 80.81 5,535.91 11107/03 86.42 84.86 Water Levels and Data over Time White Mesa Mill -Well MW 4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,620.77 5,622.33 1.56 123.6 5,550.70 12/03/03 71.63 70.07 5,557.58 01/15/04 64.75 63.19 5,558.80 02/10104 63.53 61.97 5,560.08 03/28/04 62.25 60.69 5,560.55 04/12/04 61.78 60.22 5,561.06 05/13/04 61.27 59.71 5,561.48 06/18/04 60.85 59.29 5,561.86 07/28/04 60.47 58.91 5,529.17 08/30104 93.16 91.60 5,536.55 09/16104 85.78 84.22 5,529.00 10/11/04 93.33 91.77 5,541.55 11/16/04 80.78 79.22 5,541.12 12/22/04 81.21 79.65 5,540.59 01/18/05 81.74 80.18 ~ 5,542.85 02/28/05 79.48 77.92 5,537.91 03/15/05 84.42 82.86 5,548.67 04/26105 73.66 72.10 5,549.53 05/24/05 72.80 71.24 5,544.36 06/30105 77.97 76.41 5,545.16 07/29/05 77.17 75.61 5,544.67 09/12/05 77.66 76.10 5,541.28 09/27/05 81.05 79.49 5,536.96 12/07/05 85.37 83.81 5,546.49 03/08/06 75.84 74.28 5,546.15 06/13/06 76.18 74.62 5,545.15 07/18/06 77.18 75.62 5,545.91 11/17/06 76.42 74.86 5,545.90 02/27/07 76.43 74.87 5,548.16 05/02/07 74.17 72.61 5,547.20 08/13/07 75.13 73.57 5,547.20 10/10107 75.13 73.57 5,547.79 03/26108 74.54 72.98 5,545.09 06/25/08 77.24 75.68 5,550.36 08/26108 71.97 70.41 5,550.39 10/14/08 71.94 70.38 5,542.25 03/03/09 80.08 78.52 5,542.25 06/24/09 80.08 78.52 5,550.19 09/10109 72.14 70.58 5,550.94 12/11/09 71.39 69.83 5,546.08 03/11/10 76.25 74.69 5,550.98 05/11/10 71.35 69.79 5,548.33 09/29/10 74.00 72.44 5,551.01 12/21/10 71.32 69.76 Water Levels and Data over Time White Mesa Mill -Well MW 4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,620.77 5,622.33 1.56 123.6 5,547.00 02/28111 75.33 73.77 5,557.54 06/21111 64.79 63.23 5,551.14 09/20/11 71.19 69.63 5,550.32 12/21111 72.01 70.45 5,551.22 03/27112 71.11 69.55 5,551.29 06/28/12 71.04 69.48 5,550.29 09/27112 72.04 70.48 Water Levels and Data over Time White Mesa Mill -Well TW 4-1 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well z 5,620.77 5,618.58 1.02 111.04 5,537.23 11108/99 81.35 80.33 5,537.38 11109/99 81.20 80.18 5,537.48 01102/00 81.10 80.08 5,537.48 01/10/00 81.10 80.08 5,537.23 01/17/00 81.35 80.33 5,537.28 01124/00 81.30 80.28 5,537.28 02/01100 81.30 80.28 5,537.18 02/07/00 81.40 80.38 5,537.48 02/14/00 81.10 80.08 5,537.48 02/23/00 81.10 80.08 5,537.58 03/01100 81.00 79.98 5,537.68 03/08/00 80.90 79.88 5,537.98 03/15/00 80.60 79.58 5,537.68 03/20/00 80.90 79.88 5,537.68 03/29/00 80.90 79.88 5,537.43 04/04/00 81.15 80.13 5,537.18 04/13/00 81.40 80.38 5,537.48 04/21100 81.10 80.08 5,537.68 04/28/00 80.90 79.88 5,537.58 05/01100 81.00 79.98 5,537.88 05/11100 80.70 79.68 5,537.58 05/15/00 81.00 79.98 5,537.88 OS/25/00 80.70 79.68 5,537.88 06/09/00 80.70 79.68 5,537.90 06/16/00 80.68 79.66 5,537.88 06/26/00 80.70 79.68 5,538.10 07/06/00 80.48 79.46 5,538.04 07/13/00 80.54 79.52 5,538.16 07/18/00 80.42 79.40 5,538.42 07/27/00 80.16 79.14 5,538.56 08/02/00 80.02 79.00 5,538.68 08/09/00 79.90 78.88 5,538.66 08/15/00 79.92 78.90 5,538.33 08/31100 80.25 79.23 5,539.18 09/01100 79.40 78.38 5,539.12 09/08/00 79.46 78.44 5,539.34 09/13/00 79.24 78.22 5,539.50 09/20/00 79.08 78.06 5,539.69 10/05/00 78.89 77.87 5,540.33 11109/00 78.25 77.23 5,540.74 12/06/00 77.84 76.82 5,542.39 01114/01 76.19 75.17 5,543.69 02/02/01 74.89 73.87 Water Levels and Data over Time White Mesa Mill -Well TW 4-1 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well z 5,620.77 5,618.58 1.02 111.04 5,544.96 03/29101 73.62 72.60 5,545.45 04/30101 73.13 72.11 5,545.89 05/31101 72.69 71.67 5,546.19 06/21101 72.39 71.37 5,546.50 07/10101 72.08 71.06 5,547.18 08/20101 71.40 70.38 5,547.59 09/19101 70.99 69.97 5,547.84 10102/01 70.74 69.72 5,548.12 11108/01 70.46 69.44 5,548.65 12/03/01 69.93 68.91 5,548.87 01103/02 69.71 68.69 5,549.37 02/06/02 69.21 68.19 5,550.00 03/26/02 68.58 67.56 5,550.22 04/09102 68.36 67.34 5,550.81 05/23/02 67.77 66.75 5,550.79 06/05/02 67.79 66.77 5,551.08 07/08/02 67.50 66.48 5,551.54 08/23/02 67.04 66.02 5,551.79 09/11102 66.79 65.77 5,552.19 10/23/02 66.39 65.37 5,552.27 11122/02 66.31 65.29 5,552.48 12/03/02 66.10 65.08 5,552.74 01109103 65.84 64.82 5,552.92 02/12/03 65.66 64.64 5,553.40 03/26/03 65.18 64.16 5,553.48 04/02/03 65.10 64.08 5,552.32 05/01103 66.26 65.24 5,550.53 06/09103 68.05 67.03 5,550.09 07/07/03 68.49 67.47 5,549.64 08/04/03 68.94 67.92 5,549.31 09/11103 69.27 68.25 5,549.58 10102/03 69.00 67.98 5,549.50 11107/03 69.08 68.06 5,550.07 12/03/03 68.51 67.49 5,551.86 01115/04 66.72 65.70 5,552.57 02/10104 66.01 64.99 5,553.63 03/28/04 64.95 63.93 5,554.04 04/12/04 64.54 63.52 5,554.60 05/13/04 63.98 62.96 5,556.28 06/18/04 62.30 61.28 5,556.61 07/28/04 61.97 60.95 5,554.21 08/30104 64.37 63.35 5,553.49 09/16/04 65.09 64.07 Water Levels and Data over Time White Mesa Mill -Well TW 4-1 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well z 5,620.77 5,618.58 1.02 111.04 5,552.53 10111/04 66.05 65.03 5,552.42 11116104 66.16 65.14 5,552.46 12/22/04 66.12 65.10 5,552.07 01118/05 66.51 65.49 5,552.21 02/28/05 66.37 65.35 5,552.26 03115/05 66.32 65.30 5,552.30 04/26105 66.28 65.26 5,552.25 05/24/05 66.33 65.31 5,552.22 06/30105 66.36 65.34 5,552.15 07/29105 66.43 65.41 5,552.47 09112/05 66.11 65.09 5,552.50 12/07/05 66.08 65.06 5,552.96 03/08/06 65.62 64.60 5,553.23 06114/06 65.35 64.33 5,557.20 07118/06 61.38 60.36 5,553.32 11/07/06 65.26 64.24 5,554.35 02/27/07 64.23 63.21 5,554.07 05/02/07 64.51 63.49 5,554.07 08114/07 64.51 63.49 5,553.88 10110107 64.70 63.68 5,555.73 03/26108 62.85 61.83 5,556.60 06/24/08 61.98 60.96 5,556.83 08/26108 61.75 60.73 5,556.87 10114/08 61.71 60.69 5,556.90 03/10109 61.68 60.66 5,556.91 06/24/09 61.67 60.65 5,556.61 09110109 61.97 60.95 5,556.78 12111/09 61.8 60.78 5,556.75 03111110 61.83 60.81 5,556.19 05111/10 62.39 61.37 5,555.26 09/29110 63.32 62.30 5,554.66 12/21110 63.92 62.90 5,554.74 02/28111 63.84 62.82 5,554.57 06/21111 64.01 62.99 5,554.13 09/20111 64.45 63.43 5,554.54 12/21/11 64.04 63.02 5,553.64 03/27112 64.94 63.92 5,553.66 06/28112 64.92 63.90 5,553.73 09/27112 64.85 63.83 Water Levels and Data over Time White Mesa Mill -Well TW 4-2 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,623.10 5,624.72 1.62 121.125 5,548.57 11108/99 76.15 74.53 5,548.57 11109/99 76.15 74.53 5,548.32 01102/00 76.40 74.78 5,548.52 01/10/00 76.20 74.58 5,548.32 01117/00 76.40 74.78 5,548.72 01124/00 76.00 74.38 5,548.62 02/01100 76.10 74.48 5,548.62 02/07/00 76.10 74.48 5,549.02 02/14/00 75.70 74.08 5,549.12 02/23/00 75.60 73.98 5,549.22 03/01100 75.50 73.88 5,549.32 03/08/00 75.40 73.78 5,549.22 03/15/00 75.50 73.88 5,549.92 03/20/00 74.80 73.18 5,549.72 03 /29/00 75.00 73.38 5,549.42 04/04/00 75.30 73.68 5,549.52 04/13/00 75.20 73.58 5,549.72 04/21100 75 .00 73.38 5,549.82 04/28/00 74.90 73.28 5,549.82 05/01100 74.90 73.28 5,550.12 05/1 1100 74.60 72.98 5,549.82 05/15/00 74.90 73.28 5,550.12 OS/25/00 74.60 72.98 5,550.12 06/09/00 74.60 72.98 5,550.22 06/16/00 74.50 72.88 5,550.07 06/26/00 74.65 73 .03 5,550.17 07/06/00 74.55 72.93 5,550.17 07/13/00 74.55 72.93 5,550.18 07/18/00 74.54 72.92 5,550.33 07/27/00 74.39 72.77 5,550.38 08/02/00 74.34 72.72 5,550.40 08/09/00 74.32 72.70 5,550.42 08/15/00 74.30 72.68 5,550.54 08/31100 74.18 72.56 5,550.87 09/08/00 73 .85 72.23 5,550.97 09/13/00 73.75 72.13 5,551.04 09/20/00 73.68 72.06 5,545.83 10/05/00 78.89 77.27 5,546.47 11109/00 78.25 76.63 5,546.88 12/06/00 77.84 76.22 5,552.18 01126/01 72.54 70.92 5,552.20 02/02/01 72.52 70.90 5,551.10 03/29/01 73.62 72.00 Water Levels and Data over Time White Mesa Mill -Well TW 4-2 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,623.10 5,624.72 1.62 121.125 5,551.59 04/30101 73.13 71.51 5,552.03 05/31101 72.69 71.07 5,552.33 06/21101 72.39 70.77 5,552.64 07110101 72.08 70.46 5,553.32 08/20101 71.40 69.78 5,553.73 09119/01 70.99 69.37 5,553.98 10102/01 70.74 69.12 5,554.14 11108/01 70.58 68.96 5,554.79 12/03/01 69.93 68.31 5,554.74 01103/02 69.98 68.36 5,554.91 02/06102 69.81 68.19 5,555.15 03/26102 69.57 67.95 5,555.39 04/09/02 69.33 67.71 5,555.73 05/23/02 68.99 67.37 5,555.79 06105/02 68.93 67.31 5,555.91 07/08/02 68.81 67.19 5,556.04 08/23/02 68.68 67.06 5,556.25 09111102 68.47 66.85 5,556.72 10/23/02 68.00 66.38 5,556.42 11/22/02 68.30 66.68 5,557.01 12/03/02 67.71 66.09 5,557.20 01109/03 67.52 65.90 5,557.35 02112/03 67.37 65.75 5,557.83 03/26103 66.89 65.27 5,557.87 04/02/03 66.85 65.23 5,553.71 05/01103 71.01 69.39 5,548.98 06109/03 75.74 74.12 5,548.14 07/07/03 76.58 74.96 5,547.75 08/04/03 76.97 75.35 5,547.22 09/11103 77.50 75.88 5,547.68 10102/03 77.04 75.42 5,547.52 11107/03 77.20 75.58 5,548.29 12/03/03 76.43 74.81 5,554.00 01115/04 70.72 69.10 5,555.46 02110104 69.26 67.64 5,556.90 03/28/04 67.82 66.20 5,557.49 04112/04 67.23 65.61 5,558.07 05113/04 66.65 65.03 5,558.19 06118/04 66.53 64.91 5,559.00 07/28/04 65.72 64.10 5,554.26 08/30104 70.46 68.84 5,551.97 09116104 72.75 71.13 5,549.65 10111104 75.07 73.45 Water Levels and Data over Time White Mesa Mill -Well TW 4-2 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,623.10 5,624.72 1.62 121.125 5,549.89 11116/04 74.83 73.21 5,550.37 12/22/04 74.35 72.73 5,549.95 01118/05 74.77 73.15 5,550.09 02/28/05 74.63 73.01 5,550.13 03115/05 74.59 72.97 5,550.18 04/26/05 74.54 72.92 5,550.32 05/24/05 74.40 72.78 5,550.21 06/30105 74.51 72.89 5,550.11 07/29/05 74.61 72.99 5,550.33 09/12/05 74.39 72.77 5,550.29 12/07/05 74.43 72.81 5,551.30 03/08/06 73.42 71.80 5,551.42 06/14/06 73.3 71.68 5,550.52 07118/06 74.20 72.58 5550.52 11107/06 74.20 72.58 5552.89 02/27/07 71.83 70.21 5,552.06 05/02/07 72.66 71.04 5,552.02 08/14/07 72.7 71.08 5,552.20 10/10107 72.52 70.90 5,554.58 03/26/08 70.14 68.52 5,555.23 06/24/08 69.49 67.87 5,555.29 08/26/08 69.43 67.81 5,555.43 10114/08 69.29 67.67 5,555.73 03110109 68.99 67.37 5,556.25 06/24/09 68.47 66.85 5,555.94 09/10109 68.78 67.16 5,556.53 12/11109 68.19 66.57 5,557.87 03/1111 0 66.85 65.23 5,557.63 05111110 67.09 65.47 5,557.24 09/29110 67.48 65.86 5,557.00 12/21110 67.72 66.10 5,557.61 02/28111 67.11 65.49 5,557.58 06/21111 67.14 65.52 5,557.46 09/20111 67.26 65.64 5,557.84 12/21111 66.88 65.26 5,557.86 03/27112 66.86 65.24 5,557.87 06/28112 66.85 65.23 5,557.46 09/27112 67.26 65.64 Water Levels and Data over Time White Mesa Mill -Well TW 4-3 Total or Measuring Measured Total Water Land Point Depth to Depth to Elevation Surface Elevation Length Of Date Of Water Water (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Total Depth Of Well 5,631.21 5,632.23 1.02 141 5,565.78 11129/99 66.45 65.43 5,566.93 01102/00 65.30 64.28 5,567.03 01110/00 65.20 64.18 5,566.83 01117/00 65.40 64.38 5,567.13 01124/00 65.10 64.08 5,567.33 02/01/00 64.90 63.88 5,567.13 02/07/00 65.10 64.08 5,567.43 02/14/00 64.80 63.78 5,567.63 02/23/00 64.60 63.58 5,567.73 03/01100 64.50 63.48 5,567.83 03/08/00 64.40 63.38 5,567.70 03/15/00 64.53 63.51 5,568.03 03/20/00 64.20 63.18 5,567.93 03/29/00 64.30 63.28 5,567.63 04/04/00 64.60 63.58 5,567.83 04/13/00 64.40 63.38 5,568.03 04/21100 64.20 63.18 5,568.23 04/28/00 64.00 62.98 5,568.13 05/01100 64.10 63.08 5,568.53 05/11100 63.70 62.68 5,568.23 05/15/00 64.00 62.98 5,568.53 OS/25/00 63.70 62.68 5,568.61 06/09/00 63.62 62.60 5,568.69 06/16/00 63.54 62.52 5,568.45 06/26/00 63.78 62.76 5,568.61 07/06/00 63.62 62.60 5,568.61 07/06/00 63.62 62.60 5,568.49 07/13/00 63.74 62.72 5,568.55 07/18/00 63.68 62.66 5,568.65 07/27/00 63.58 62.56 5,568.73 08/02/00 63.50 62.48 5,568.77 08/09/00 63.46 62.44 5,568.76 08/16/00 63.47 62.45 5,568.95 08/31100 63.28 62.26 5,568.49 09/08/00 63.74 62.72 5,568.67 09/13/00 63.56 62.54 5,568.96 09/20/00 63.27 62.25 5,568.93 10/05/00 63.3 62.28 5,569.34 11109/00 62.89 61.87 5,568.79 12/06/00 63.44 62.42 5,569.11 01103/01 63.12 62.10 5,569.75 02/09/01 62.48 61.46 5,570.34 03/28/01 61.89 60.87 Water Levels and Data over Time White Mesa Mill -Well TW 4-3 Total or Measuring Measured Total Water Land Point Depth to Depth to Elevation Surface Elevation Length Of Date Of Water Water (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Total Depth Of Well 5,631.21 5,632.23 1.02 141 5,570.61 04/30101 61.62 60.60 5,570.70 05/31101 61.53 60.51 5,570.88 06/21101 61.35 60.33 5,571.02 07/10101 61.21 60.19 5,571.70 08/20101 60.53 59.51 5,572.12 09/19/01 60.11 59.09 5,572.08 10102/01 60.15 59.13 5,572.78 11/08/01 59.45 58.43 5,573.27 12/03/01 58.96 57.94 5,573.47 01103/02 58.76 57.74 5,573.93 02/06102 58.30 57.28 5,574.75 03/26102 57.48 56.46 5,574.26 04/09/02 57.97 56.95 5,575.39 05/23/02 56.84 55.82 5,574.84 06105/02 57.39 56.37 5,575.33 07/08/02 56.90 55.88 5,575.79 08/23/02 56.44 55.42 5,576.08 09/11102 56.15 55.13 5,576.30 10/23/02 55.93 54.91 5,576.35 11122/02 55.88 54.86 5,576.54 12/03/02 55.69 54.67 5,576.96 01109/03 55.27 54.25 5,577.11 02/12/03 55.12 54.10 5,577.61 03/26103 54.62 53.60 5,572.80 04/02/03 59.43 58.41 5,577.89 05/01103 54.34 53.32 5,577.91 06109/03 54.32 53.30 5,577.53 07/07/03 54.70 53.68 5,577.50 08/04/03 54.73 53.71 5,577.71 09/11103 54.52 53.50 5,577.31 10102/03 54.92 53.90 5,577.33 11107/03 54.90 53.88 5,577.34 12/03/03 54.89 53.87 5,578.24 01115/04 53.99 52.97 5,578.38 02/10104 53.85 52.83 5,578.69 03/28/04 53.54 52.52 5,579.15 04/12/04 53.08 52.06 5,579.47 05/13/04 52.76 51.74 5,579.53 06/18/04 52.70 51.68 5,580.17 07/28/04 52.06 51.04 5,580.20 08/30104 52.03 51.01 5,580.26 09/16104 51.97 50.95 5,580.12 10/11104 52.11 51.09 Water Levels and Data over Time White Mesa Mill -Well TW 4-3 Total or Measuring Measured Total Water Land Point Depth to Depth to Elevation Surface Elevation Length Of Date Of Water Water (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Total Depth Of Well 5,631.21 5,632.23 1.02 141 5,579.93 11116104 52.30 51.28 5,580.07 12/22/04 52.16 51.14 5,579.80 01118/05 52.43 51.41 5,580.35 02/28/05 51.88 50.86 5,580.57 03115/05 51.66 50.64 5,580.86 04/26105 51.37 50.35 5,581.20 05/24/05 51.03 50.01 5,581.51 06/30105 50.72 49.70 5,581.55 07/29105 50.68 49.66 5,581.68 09112/05 50.55 49.53 5,581.83 12/07/05 50.4 49.38 5,564.92 03/08/06 67.31 66.29 5,582.73 06/13/06 49.50 48.48 5,582.33 07/18/06 49.90 48.88 5,582.75 11107/06 49.48 48.46 5583.35 02/27/07 48.88 47.86 5,559.57 05/02/07 72.66 71.64 5,583.29 08114/07 48.94 47.92 5,583.49 10110107 48.74 47.72 5,584.95 03/26108 47.28 46.26 5,584.59 06/24/08 47.64 46.62 5,584.55 08126108 47.68 46.66 5,584.03 10114/08 48.2 47.18 5,583.64 03/03/09 48.59 47.57 5,587.34 06/24/09 44.89 43.87 5,582.90 09110109 49.33 48.31 5,583.27 12111109 48.96 47.94 5,583.63 03/11110 48.6 47.58 5,583.82 05111110 48.41 47.39 5,583.51 09/29/10 48.72 47.70 5,582.86 12/21110 49.37 48.35 5,582.60 02/28/11 49.63 48.61 5,590.00 06/21111 42.23 41.21 5,582.70 09/20/11 49.53 48.51 5,583.05 12/21111 49.18 48.16 5,581.93 03/27/12 50.30 49.28 5,582.03 06/28112 50.20 49.18 5,582.08 09/27112 50.15 49.13 Water Levels and Data over Time White Mesa Mill -Well TW 4-4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,612.301 5,613.485 1.184 114.5 5,512.145 05/25/00 101.34 100.16 5,518.985 06109/00 94.50 93.32 5,512.145 06/16100 101.34 100.16 5,517.465 06/26100 96.02 94.84 5,520.145 07/06100 93.34 92.16 5,521.435 07/13/00 92.05 90.87 5,522.005 07118/00 91.48 90.30 5,522.945 07/27/00 90.54 89.36 5,523.485 08/02/00 90.00 88.82 5,523.845 08/09/00 89.64 88.46 5,523.885 08115/00 89.60 88.42 5,524.555 09/01100 88.93 87.75 5,513.235 09/08/00 100.25 99.07 5,516.665 09113/00 96.82 95.64 5,519.085 09/20100 94.40 93.22 5,522.165 10105/00 91.32 90.14 5,524.665 11109/00 88.82 87.64 5,518.545 12/06100 94.94 93.76 5,527.695 01103/01 85.79 84.61 5,529.085 02/09/01 84.40 83.22 5,529.535 03 /27/01 83 .95 82.77 5,530.235 04/30101 83.25 82.07 5,530.265 05 /31101 83.22 82.04 5,534.405 06/22/01 79.08 77.90 5,533.145 07110101 80.34 79.16 5,534.035 08/20101 79.45 78.27 5,534.465 09119/01 79.02 77.84 5,533.285 10102/01 80.20 79.02 5,533.865 11108/01 79.62 78.44 5,534.275 12/03/01 79.21 78.03 5,534.715 01103 /02 78.77 77.59 5,535.435 02/06102 78.05 76.87 5,536.445 03 /26102 77.04 75.86 5,536.405 04/09/02 77.08 75.90 5,537.335 05 /23 /02 76.15 74.97 5,537.325 06105 /02 76.16 74.98 5,537.975 07/08/02 75 .51 74.33 5,538.825 08/23 /02 74.66 73.48 5,539.275 0911 1102 74.21 73.03 5,539.765 10/23 /02 73.72 72.54 5,540.205 11122/02 73.28 72.10 5,540.295 12/03 /02 73 .19 72 .01 5,540.795 01109/03 72.69 71.51 Water Levels and Data over Time White Mesa Mill -Well TW 4-4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,612.301 5,613.485 1.184 114.5 5,540.985 02/12/03 72.50 71.32 5,541.675 03 /26103 71.81 70.63 5,541.765 04/02/03 71.72 70.54 5,541.885 05/01103 71.60 70.42 5,542.025 06109/03 71.46 70.28 5,541.925 07/07/03 71.56 70.38 5,541.885 08/04/03 71.60 70.42 5,541.825 09111103 71.66 70.48 5,541.885 10102/03 71.60 70.42 5,541.995 11107/03 71.49 70.31 5,542.005 12/03/03 71.48 70.30 5,542.555 01115/04 70.93 69.75 5,542.705 02110104 70.78 69.60 5,543.225 03 /28/04 70.26 69.08 5,543.555 04112/04 69.93 68.75 5,543.865 05113/04 69.62 68.44 5,543.915 06118/04 69.57 68.39 5,544.655 07/28/04 68.83 67.65 5,544.795 08/30104 68.69 67.51 5,544.845 09116104 68.64 67.46 5,544.705 10111104 68.78 67.60 5,544.525 11116/04 68.96 67.78 5,544.625 12/22/04 68.86 67.68 5,544.305 01118/05 69.18 68.00 5,544.585 02/28/05 68.90 67.72 5,544.685 03115/05 68.80 67.62 5,544.675 04/26105 68.81 67.63 5,544.785 05/24/05 68.70 67.52 5,544.795 06/30105 68.69 67.51 5,544.775 07/29/05 68.71 67.53 5,545.005 09112/05 68.48 67.30 5,545.225 12/07/05 68.26 67.08 5,545.735 03/08/06 67.75 66.57 5,545.785 06114/06 67.70 66.52 5,545.855 07118/06 67.63 66.45 5,545.805 11107/06 67.68 66.50 5546.675 02/27/07 66.81 65.63 5,546.535 05/02/07 66.95 65.77 5,547.155 08115/07 66.33 65.15 5,547.215 10/10107 66.27 65.09 5,548.305 03/26108 65.18 64.00 5,548.865 06/24/08 64.62 63.44 5,549.235 08/26108 64.25 63.07 Water Levels and Data over Time White Mesa Mill -Well TW 4-4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,612.301 5,613.485 1.184 114.5 5,549.305 10114/08 64.l8 63.00 5,549.725 03/03/09 63.76 62.58 5,549.905 06/24/09 63.58 62.40 5,549.695 09110109 63.79 62.61 5,549.865 12111109 63.62 62.44 5,545.60 03111110 67.89 66.71 5,530.88 05111110 82.61 81.43 5,545.24 09/29110 68.25 67.07 5,533.66 12/21110 79.83 78.65 5,544.44 02/28111 69.05 67.87 5,543.73 06/21111 69.76 68.58 5,540.48 09/20111 73.01 71.83 5,544.36 12/21111 69.13 67.95 5,543.48 03/27112 70.01 68.83 5,543.49 06/28112 70.00 68.82 5,543.36 09/27112 70.13 68.95 Water Levels and Data over Time White Mesa Mill -Well TW 4-5 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,638.75 5,640.70 1.95 121.75 5,579.30 01102/00 61.40 59.45 5,579.60 01110100 61.10 59.15 5,579.35 01117/00 61.35 59.40 5,579.60 01124/00 61.10 59.15 5,579.50 02/01100 61.20 59.25 5,579.50 02/07/00 61.20 59.25 5,579.90 02114/00 60.80 58.85 5,579.90 02/23/00 60.80 58.85 5,580.20 03/01100 60.50 58.55 5,580.00 03/08/00 60.70 58.75 5,580.04 03/15/00 60.66 58.71 5,580.70 03/20100 60.00 58.05 5,580.30 03/29/00 60.40 58.45 5,580.00 04/04/00 60.70 58.75 5,580.20 04113/00 60.50 58.55 5,580.40 04/21100 60.30 58.35 5,580.50 04/28/00 60.20 58.25 5,580.50 05/01100 60.20 58.25 5,580.90 05111100 59.80 57.85 5,580.50 05115/00 60.20 58.25 5,580.75 05/25/00 59.95 58.00 5,580.80 06/09/00 59.90 57.95 5,580.92 06116/00 59.78 57.83 5,580.80 06/26/00 59.90 57.95 5,580.90 07/06/00 59.80 57.85 5,581.05 07/13/00 59.65 57.70 5,580.90 07118/00 59.80 57.85 5,581.05 07/27/00 59.65 57.70 5,581.06 08/02/00 59.64 57.69 5,581.08 08/09/00 59.62 57.67 5,581.07 08116/00 59.63 57.68 5,581.25 08/31100 59.45 57.50 5,581.32 09/08/00 59.38 57.43 5,581.34 09113/00 59.36 57.41 5,581.41 09/20100 59.29 57.34 5,581.37 10105/00 59.33 57.38 5,581.66 11109/00 59~04 57.09 5,581.63 12/06/00 59.07 57.12 5,581.92 01103/01 58.78 56.83 5,582.20 02/09/01 58.50 56.55 5,582.54 03/28/01 58.16 56.21 5,582.72 04/30101 57.98 56.03 5,582.72 05/31/01 57.98 56.03 Water Levels and Data over Time White Mesa Mill -Well TW 4-5 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,638.75 5,640.70 1.95 121.75 5,582.81 06/22/01 57.89 55.94 5,582.92 07/10101 57.78 55.83 5,583.17 08/20101 57.53 55.58 5,583.28 09/19/01 57.42 55.47 5,583.36 10102/01 57.34 55.39 5,583.49 11108/01 57.21 55.26 5,583.84 12/03/01 56.86 54.91 5,583.79 01103/02 56.91 54.96 5,583.96 02/06102 56.74 54.79 5,584.39 03/26102 56.31 54.36 5,584.12 04/09/02 56.58 54.63 5,584.55 05/23/02 56.15 54.20 5,584.42 06105/02 56.28 54.33 5,583.65 07/08/02 57.05 55.10 5,584.90 08/23/02 55.80 53.85 5,585.02 09/11102 55.68 53.73 5,585.20 10/23/02 55.50 53.55 5,585.15 11122/02 55.55 53.60 5,585.42 12/03/02 55.28 53.33 5,585.65 01109/03 55.05 53.10 5,585.65 02/12/03 55.05 53.10 5,585.92 03/26103 54.78 52.83 5,586.22 04/02/03 54.48 52.53 5,586.01 05/01103 54.69 52.74 5,584.81 06109/03 55.89 53.94 5,584.34 07/07/03 56.36 54.41 5,584.40 08/04/03 56.30 54.35 5,583.88 09/11103 56.82 54.87 5,583.57 10102/03 57.13 55.18 5,583.39 11107/03 57.31 55.36 5,583.97 12/03/03 56.73 54.78 5,585.28 01115/04 55.42 53.47 5,585.50 02/10104 55.20 53.25 5,585.87 03/28/04 54.83 52.88 5,586.20 04/12/04 54.50 52.55 5,586.45 05/13/04 54.25 52.30 5,586.50 06/18/04 54.20 52.25 5,587.13 07/28/04 53.57 51.62 5,586.22 08/30104 54.48 52.53 5,585.69 09/16104 55.01 53.06 5,585.17 10/11104 55.53 53.58 5,584.64 11116/04 56.06 54.11 5,584.77 12/22/04 55.93 53.98 Water Levels and Data over Time White Mesa Mill -Well TW 4-5 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,638.75 5,640.70 l.95 12l.75 5,584.65 01118/05 56.05 54.10 5,584.98 02/28/05 55 .72 53.77 5,585.15 03115/05 55 .55 53.60 5,586.25 04/26/05 54.45 52.50 5,586.79 05 /24/05 53.91 51.96 5,586.52 06/30105 54.18 52.23 5,586.03 07/29/05 54.67 52.72 5,586.05 09112/05 54.65 52.70 5,585.80 12/07/05 54.90 52.95 5,587.06 03 /08/06 53.64 5l.69 5,585.90 06113/06 54.80 52.85 5,585.32 07118/06 55.38 53.43 5,585.35 11107/06 55.35 53.40 5585.81 02/27/07 54.89 52.94 5,585.20 05/02/07 55.50 53.55 5,586.66 08/14/07 54.04 52.09 5,586.80 10110107 53.90 5l.95 5,588.48 03/26/08 52.22 50.27 5,586.51 06/24/08 54.19 52 .24 5,586.45 08/26/08 54.25 52.30 5,585.40 10114/08 55.3 53.35 5,584.80 03 /03/09 55.9 53.95 5,584.73 06/24/09 55.97 54.02 5,584.36 09110109 56.34 54.39 5,585.02 12111109 55.68 53.73 5,585.66 03111110 55.04 53.09 5,584.86 05111110 55.84 53.89 5,584.55 09/29110 56.15 54.20 5,584.17 12/21110 56.53 54.58 5,583.55 02/28111 57.15 55.20 5,584.72 06/21111 55.98 54.03 5,584.62 09/20111 56.08 54.13 5,585.04 11121111 55.66 53.71 5,583.89 03/27112 56.81 54.86 5,583.92 06/28112 56.78 54.83 5,583.89 09/27112 56.81 54.86 Water Levels and Data over Time White Mesa Mill -Well TW 4-6 Total or Measuring Measured Total Total Water Land Point Depth to Depth to Depth Of Elevation Surface Elevation Length Of Date Of Water Water Well (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) (blw.LSD) 5,607.33 5,608.78 1.450 98.55 5,522.28 05/25/00 86.50 85.05 5,521.51 06109100 87.27 85.82 5,522.35 06116100 86.43 84.98 5,522.14 06/26100 86.64 85.19 5,522.25 07/06100 86.53 85.08 5,522.13 07113/00 86.65 85.20 5,522.17 07118/00 86.61 85.16 5,522.26 07/25/00 86.52 85.07 5,522.31 08/02/00 86.47 85.02 5,522.33 08/09100 86.45 85.00 5,522.35 08115/00 86.43 84.98 5,522.40 08/31100 86.38 84.93 5,522.40 09108/00 86.38 84.93 5,522.45 09/13/00 86.33 84.88 5,522.53 09/20100 86.25 84.80 5,522.39 10105/00 86.39 84.94 5,522.42 11109100 86.36 84.91 5,522.29 12/06100 86.49 85.04 5,522.63 01/03/01 86.15 84.70 5,522.72 02/09101 86.06 84.61 5,522.90 03/26101 85.88 84.43 5,522.70 04/30101 86.08 84.63 5,522.89 05/31101 85.89 84.44 5,522.88 06/20101 85.90 84.45 5,522.96 07110101 85.82 84.37 5,523.10 08/20101 85.68 84.23 5,523.23 09119101 85.55 84.10 5,523.21 10102/01 85.57 84.12 5,523.25 11108/01 85.53 84.08 5,523.46 12/03/01 85.32 83.87 5,523.36 01103/02 85.42 83.97 5,523.50 02/06102 85.28 83.83 5,523.94 03/26102 84.84 83.39 5,523.75 04/09102 85.03 83.58 5,524.23 05/23/02 84.55 83.10 5,523.98 06105/02 84.80 83.35 5,524.31 07/08/02 84.47 83.02 5,524.36 08/23/02 84.42 82.97 5,524.49 09111102 84.29 82.84 5,524.71 10/23/02 84.07 82.62 5,524.60 11/22/02 84.18 82.73 5,524.94 12/03/02 83.84 82.39 5,525.10 01109103 83.68 82.23 Water Levels and Data over Time White Mesa Mill -Well TW 4-6 Total or Measuring Measured Total Total Water Land Point Depth to Depth to Depth Of Elevation Surface Elevation Length Of Date Of Water Water Well (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) (blw.LSD) 5,607.33 5,608.78 1.450 98.55 5,525.15 02112/03 83.63 82.18 5,525.35 03/26103 83.43 81.98 5,525.68 04/02/03 83.10 81.65 5,525.74 05/01103 83.04 81.59 5,525.98 06109/03 82.80 81.35 5,526.04 07/07/03 82.74 81.29 5,526.07 08/04/03 82.71 81.26 5,526.42 09111103 82.36 80.91 5,526.30 10102/03 82.48 81.03 5,526.41 11107/03 82.37 80.92 5,526.46 12/03/03 82.32 80.87 5,526.83 01115/04 81.95 80.50 5,526.81 02110104 81.97 80.52 5,527.14 03/28/04 81.64 80.19 5,527.39 04112/04 81.39 79.94 5,527.64 05/13/04 81.14 79.69 5,527.70 06118/04 81.08 79.63 5,528.16 07/28/04 80.62 79.17 5,528.30 08/30104 80.48 79.03 5,528.52 09116104 80.26 78.81 5,528.71 10111104 80.07 78.62 5,528.74 11116104 80.04 78.59 5,529.20 12/22/04 79.58 78.13 5,528.92 01118/05 79.86 78.41 5,529.51 02/28/05 79.27 77.82 5,529.74 03115/05 79.04 77.59 5,529.96 04/26105 78.82 77.37 5,530.15 05/24/05 78.63 77.18 5,530.35 06/30105 78.43 76.98 5,530.47 07/29/05 78.31 76.86 5,530.95 09112/05 77.83 76.38 5,531.50 12/07/05 77.28 75.83 5,532.43 03/08/06 76.35 74.90 5,533.49 06113/06 75.29 73.84 5,532.58 07118/06 76.20 74.75 5,532.88 11107/06 75.90 74.45 5534.09 02/27/07 74.69 73.24 5,534.04 05/02/07 74.74 73.29 5,534.43 08114/07 74.35 72.90 5,554.54 10110107 54.24 52.79 5,535.40 03/26108 73.38 71.93 5,535.55 06/24/08 73.23 71.78 5,535.90 08/26108 72.88 71.43 Water Levels and Data over Time White Mesa Mill -Well TW 4-6 Total or Measuring Measured Total Total Water Land Point Depth to Depth to Depth Of Elevation Surface Elevation Length Of Date Of Water Water Well (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) (blw.LSD) 5,607.33 5,608.78 1.450 98.55 5,535.87 10114/08 72.91 71.46 5,536.42 03110109 72.36 70.91 5,536.71 06/24/09 72.07 70.62 5,536.83 09110109 71.95 70.50 5,537.35 12111109 71.43 69.98 5,537.93 03111110 70.85 69.40 5,538.14 05111110 70.64 69.19 5,538.03 09/29/10 70.75 69.30 5,538.04 12/21110 70.74 69.29 5,537.98 02/28111 70.8 69.35 5,538.46 06/21111 70.32 68.87 5,538.37 09/20111 70.41 68.96 5,538.87 12/21111 69.91 68.46 5,538.73 03/27112 70.05 68.60 5,538.80 06/28112 69.98 68.53 5,539.04 09/27112 69.74 68.29 Water Levels and Data over Time White Mesa Mill -Well TW 4-7 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Depth Elevation Surface Elevation Length Of Date Of Water Water Of Well (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) (blw.LSD) 5,619.87 5,621.07 1.20 119.8 5,552.37 11129/99 68.70 67.50 5,553.57 01102/00 67.50 66.30 5,553.87 01/10/00 67.20 66.00 5,553.72 01/17/00 67.35 66.15 5,553.97 01124/00 67.10 65.90 5,553.87 02/01100 67.20 66.00 5,553.87 02/07/00 67.20 66.00 5,554.17 02/14/00 66.90 65.70 5,554.27 02/23/00 66.80 65.60 5,554.37 03/01100 66.70 65.50 5,554.37 03/08/00 66.70 65.50 5,554.27 03/15/00 66.80 65.60 5,554.77 03/20/00 66.30 65.10 5,554.57 03/29/00 66.50 65.30 5,554.27 04/04/00 66.80 65.60 5,554.57 04/13/00 66.50 65.30 5,554.77 04/21100 66.30 65.10 5,554.87 04/28/00 66.20 65.00 5,554.87 05/01100 66.20 65.00 5,555.27 05/11100 65.80 64.60 5,554.97 05/15/00 66.10 64.90 5,555.27 OS/25/00 65.80 64.60 5,555.33 06/09/00 65.74 64.54 5,555.45 06/16/00 65.62 64.42 5,555.22 06/26/00 65.85 64.65 5,555.45 07/06/00 65.62 64.42 5,555.40 07/13/00 65.67 64.47 5,555.45 07/18/00 65.62 64.42 5,555.59 07/27/00 65.48 64.28 5,555.65 08/02/00 65.42 64.22 5,555.70 08/09/00 65.37 64.17 5,555.74 08/16/00 65.33 64.l3 5,555.96 08/31100 65.11 63.91 5,555.87 09/08/00 65.20 64.00 5,555.95 09/13/00 65.12 63.92 5,556.05 09/20/00 65.02 63.82 5,556.06 10/05/00 65.01 63.81 5,556.17 10/12/00 64.90 63.70 5,556.20 10/19/00 64.87 63.67 5,556.22 10/23/00 64.85 63.65 5,556.36 11109/00 64.71 63.51 5,556.42 11114/00 64.65 63.45 5,556.45 11130/00 64.62 63.42 Water Levels and Data over Time White Mesa Mill -Well TW 4-7 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Depth Elevation Surface Elevation Length Of Date Of Water Water Of Well (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) (blw.LSD) 5,619.87 5,621.07 1.20 119.8 5,556.15 12/06/00 64.92 63.72 5,556.89 01114/01 64.18 62.98 5,557.07 02/09/01 64.00 62.80 5,557.62 03/29/01 63.45 62.25 5,557.51 04/30101 63.56 62.36 5,557.77 05/31101 63.30 62.10 5,557.84 06/21101 63.23 62.03 5,557.98 07110101 63.09 61.89 5,558.33 08/20101 62.74 61.54 5,558.57 09119/01 62.50 61.30 5,558.53 10102/01 62.54 61.34 5,558.62 11108/01 62.45 61.25 5,559.03 12/03/01 62.04 60.84 5,559.08 01103/02 61.99 60.79 5,559.32 02/06/02 61.75 60.55 5,559.63 03/26/02 61.44 60.24 5,559.55 04/09/02 61.52 60.32 5,560.06 OS/23/02 61.01 59.81 5,559.91 06/05/02 61.16 59.96 5,560.09 07/08/02 60.98 59.78 5,560.01 08/23/02 61.06 59.86 5,560.23 09111102 60.84 59.64 5,560.43 10/23/02 60.64 59.44 5,560.39 11122/02 60.68 59.48 5,560.61 12/03/02 60.46 59.26 5,560.89 01109/03 60.18 58.98 5,560.94 02112/03 60.13 58.93 5,561.28 03/26/03 59.79 58.59 5,561.35 04/02/03 59.72 58.52 5,546.20 05/01103 74.87 73.67 5,539.47 06/09/03 81.60 80.40 5,541.87 07/07/03 79.20 78.00 5,542.12 08/04/03 78.95 77.75 5,541.91 09111103 79.16 77.96 5,544.62 10102/03 76.45 75.25 5,542.67 11107/03 78.40 77.20 5,549.96 12/03/03 71.11 69.91 5,557.17 01115/04 63.90 62.70 5,558.65 02110104 62.42 61.22 5,559.90 03/28/04 61.17 59.97 5,560.36 04112/04 60.71 59.51 5,560.87 05113/04 60.20 59.00 5,560.95 06118/04 60.12 58.92 Water Levels and Data over Time White Mesa Mill -Well TW 4-7 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Depth Elevation Surface Elevation Length Of Date Of Water Water Of Well (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) (blw.LSD) 5,619.87 5,62l.07 l.20 119.8 5,56l.64 07/28/04 59.43 58.23 5,543.00 08/30104 78.07 76.87 5,54l.91 09116/04 79.16 77.96 5,540.08 10111104 80.99 79.79 5,546.92 11116/04 74.15 72.95 5,546.97 12/22/04 74.10 72.90 5,546.51 01118/05 74.56 73.36 5,546.66 02/28/05 74.41 73.21 5,546.81 03115/05 74.26 73.06 5,548.19 04/26/05 72.88 7l.68 5,547.11 05/24/05 73.96 72.76 5,546.98 06/30105 74.09 72.89 5,546.92 07/29105 74.15 72.95 5,547.26 09112/05 73.81 72.61 5,547.26 12/07/05 73.81 72.61 5,548.86 03/08/06 72.21 7l.01 5,548.62 06113/06 72.45 7l.25 5,550.04 07118/06 7l.03 69.83 5,548.32 11107/06 72.75 7l.55 5,550.44 02/27/07 70.63 69.43 5,549.69 05/02/07 7l.38 70.18 5,549.97 08/14/07 7l.10 69.90 5,550.30 10/10107 70.77 69.57 5,55l.92 03/26/08 69.15 67.95 5,552.94 06/24/08 68.13 66.93 5,552.34 08/26/08 68.73 67.53 5,552.61 10/14/08 68.46 67.26 5,552.81 03110109 68.26 67.06 5,553.11 06/24/09 67.96 66.76 5,552.55 09/10109 68.52 67.32 5,553.06 12/11109 68.01 66.81 5,554.64 03111110 66.43 65.23 5,554.20 05/11110 66.87 65.67 5,553.45 09/29110 67.62 66.42 5,553.40 12/21110 67.67 66.47 5,553.93 02/28111 67.14 65.94 5,553.67 06/21111 67.4 66.20 5,553.46 09/20111 67.61 66.41 5,553.78 12/21111 67.29 66.09 5,553.l7 03/27/12 67.90 66.70 5,553.21 06/28112 67.86 66.66 5,552.90 09/27112 68.17 66.97 Water Levels and Data over Time White Mesa Mill -Well TW 4-8 Total or Measuring Measured Water Land Point Depth to Total Depth Total Elevation Surface Elevation Length Of Date Of Water to Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,616.80 5,621.40 4.60 126.00 5,546.40 11129/99 75.00 70.40 5,546.20 01102/00 75.20 70.60 5,546.50 01110100 74.90 70.30 5,546.30 01117/00 75.10 70.50 5,546.60 01124/00 74.80 70.20 5,546.50 02/01100 74.90 70.30 5,546.50 02/07/00 74.90 70.30 5,546.90 02114/00 74.50 69.90 5,546.95 02/23/00 74.45 69.85 5,547.05 03/01100 74.35 69.75 5,547.05 03/08/00 74.35 69.75 5,547.10 03115/00 74.30 69.70 5,547.50 03/20100 73.90 69.30 5,547.40 03/29/00 74.00 69.40 5,547.20 04/04/00 74.20 69.60 5,547.40 04113/00 74.00 69.40 5,547.60 04/21100 73.80 69.20 5,547.70 04/28/00 73.70 69.10 5,547.70 05/01100 73.70 69.10 5,548.00 05/11100 73.40 68.80 5,547.70 05115/00 73.70 69.10 5,547.90 05/25/00 73.50 68.90 5,547.90 06109/00 73.50 68.90 5,548.00 06116100 73.40 68.80 5,547.87 06/26100 73.53 68.93 5,547.95 07/06100 73.45 68.85 5,547.96 07113/00 73.44 68.84 5,547.95 07/18/00 73.45 68.85 5,548.11 07/27/00 73.29 68.69 5,548.15 08/02/00 73.25 68.65 5,548.17 08/09/00 73.23 68.63 5,548.16 08115/00 73.24 68.64 5,548.40 08/31100 73.00 68.40 5,548.50 09/08/00 72.90 68.30 5,548.62 09113/00 72.78 68.18 5,548.75 09/20100 72.65 68.05 5,548.76 10105/00 72.64 68.04 5,549.00 11109/00 72.40 67.80 5,548.85 12/06100 72.55 67.95 5,549.47 01103/01 71.93 67.33 5,549.89 02/09/01 71.51 66.91 5,550.37 03/27/01 71.03 66.43 5,550.50 04/30101 70.90 66.30 Water Levels and Data over Time White Mesa Mill -Well TW 4-8 Total or Measuring Measured Water Land Point Depth to Total Depth Total Elevation Surface Elevation Length Of Date Of Water to Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,616.80 5,621.40 4.60 126.00 5,550.68 05/31101 70.72 66.12 5,550.68 06/20101 70.72 66.12 5,551.02 07/10101 70.38 65.78 5,551.32 08/20101 70.08 65.48 5,551.49 09/19/01 69.91 65.31 5,551.64 10102/01 69.76 65.16 5,551.81 11108/01 69.59 64.99 5,552.22 12/03/01 69.l8 64.58 5,552.l6 01103/02 69.24 64.64 5,552.38 02/06/02 69.02 64.42 5,552.85 03/26/02 68.55 63.95 5,552.83 04/09/02 68.57 63.97 5,553.20 05/23/02 68.20 63.60 5,553.l6 06/05/02 68.24 63.64 5,553.32 07/08/02 68.08 63.48 5,553.49 08/23/02 67.91 63.31 5,553.69 09/11102 67.71 63.11 5,554.09 10/23/02 67.31 62.71 5,554.02 11122/02 67.38 62.78 5,554.23 12/03/02 67.17 62.57 5,554.43 01109/03 66.97 62.37 5,554.42 02/12/03 66.98 62.38 5,554.71 03/26/03 66.69 62.09 5,554.83 04/02/03 66.57 61.97 5,552.21 05/01103 69.19 64.59 5,547.93 06/09/03 73.47 68.87 5,546.97 07/07/03 74.43 69.83 5,546.58 08/04/03 74.82 70.22 5,546.24 09/11103 75.16 70.56 5,546.38 10102/03 75.02 70.42 5,546.40 11107/03 75.00 70.40 5,546.59 12/03/03 74.81 70.21 5,551.29 01115/04 70.l1 65.51 5,552.69 02/10104 68.71 64.11 5,554.06 03/28/04 67.34 62.74 5,554.52 04/12/04 66.88 62.28 5,555.06 05/13/04 66.34 61.74 5,555.l1 06/18/04 66.29 61.69 5,555.88 07/28/04 65.52 60.92 5,552.97 08/30104 68.43 63.83 5,550.65 09/16/04 70.75 66.15 5,548.40 10/11104 73.00 68.40 5,548.28 11116/04 73.l2 68.52 Water Levels and Data over Time White Mesa Mill -Well TW 4-8 Total or Measuring Measured Water Land Point Depth to Total Depth Total Elevation Surface Elevation Length Of Date Of Water to Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,616.80 5,621.40 4.60 126.00 5,548.80 12/22/04 72.60 68.00 5,548.43 01118/05 72.97 68.37 5,548.61 02/28/05 72.79 68.19 5,548.64 03115/05 72.76 68.16 5,548.65 04/26/05 72.75 68.15 5,548.85 05/24/05 72.55 67.95 5,548.73 06/30105 72.67 68.07 5,548.62 07/29/05 72.78 68.18 5,548.80 09112/05 72.60 68.00 5,548.71 12/07/05 72.69 68.09 5,549.72 03/08/06 71.68 67.08 5,549.70 06113/06 71.70 67.10 5,549.70 07118/06 71.70 67.10 5,549.65 11107/06 71.75 67.15 5,551.11 02/27/07 70.29 65.69 5,550.20 05/02/07 71.20 66.60 5,550.59 08114/07 70.81 66.21 5,550.76 10110107 70.64 66.04 5,551.95 03/26/08 69.45 64.85 5,552.36 06/24/08 69.04 64.44 5,552.50 08/26/08 68.9 64.30 5,552.56 10114/08 68.84 64.24 5,552.91 03/03/09 68.49 63.89 5,553.27 06/24/09 68.13 63.53 5,553.12 09110109 68.28 63.68 5,553.63 12111109 67.77 63.17 5,554.65 03111110 66.75 62.15 5,554.57 05111110 66.83 62.23 5,554.34 09/29/10 67.06 62.46 5,554.09 12/21110 67.31 62.71 5,554.50 02/28/11 66.9 62.30 5,554.79 06/21111 66.61 62.01 5,554.63 09/20111 66.77 62.17 5,555.01 12/21111 66.39 61.79 5,554.85 03/27112 66.55 61.95 5,554.90 06/28112 66.50 61.90 5,554.85 09/27112 66.55 61.95 Water Levels and Data over Time White Mesa Mill -Well TW 4-9 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,636.11 5,637.59 1.48 121.33 5,577.09 12/20/99 60.50 59.02 5,577.09 01102/00 60.50 59.02 5,577.29 01110/00 60.30 58.82 5,577.09 01117/00 60.50 59.02 5,577.39 01124/00 60.20 58.72 5,577.29 02/01100 60.30 58.82 5,577.19 02/07/00 60.40 58.92 5,577.69 02114/00 59.90 58.42 5,577.69 02/23/00 59.90 58.42 5,577.79 03/01100 59.80 58.32 5,577.79 03/08/00 59.80 58.32 5,577.89 03115/00 59.70 58.22 5,568.49 03/20/00 69.10 67.62 5,578.14 03/29/00 59.45 57.97 5,577.84 04/04/00 59.75 58.27 5,578.04 04113/00 59.55 58.07 5,578.24 04/21100 59.35 57.87 5,578.39 04/28/00 59.20 57.72 5,578.39 05/01100 59.20 57.72 5,578.79 05111100 58.80 57.32 5,578.39 05115/00 59.20 57.72 5,578.79 OS/25/00 58.80 57.32 5,578.81 06/09/00 58.78 57.30 5,578.89 06116/00 58.70 57.22 5,578.74 06/26/00 58.85 57.37 5,578.86 07/06/00 58.73 57.25 5,578.87 07113/00 58.72 57.24 5,578.84 07118/00 58.75 57.27 5,579.03 07/27/00 58.56 57.08 5,579.03 08/02/00 58.56 57.08 5,579.05 08/09/00 58.54 57.06 5,579.04 08115/00 58.55 57.07 5,579.25 08/31100 58.34 56.86 5,579.35 09/08/00 58.24 56.76 5,579.40 09113/00 58.19 56.71 5,579.46 09/20/00 58.13 56.65 5,579.44 10/05/00 58.15 56.67 5,579.79 11109/00 57.80 56.32 5,579.73 12/06/00 57.86 56.38 5,580.01 01103/01 57.58 56.10 5,580.30 02/09/01 57.29 55.81 5,580.66 03/27/01 56.93 55.45 5,580.75 04/30/01 56.84 55.36 Water Levels and Data over Time White Mesa Mill -Well TW 4-9 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,636.11 5,637.59 1.48 121.33 5,581.04 05/31101 56.55 55.07 5,581.12 06/21101 56.47 54.99 5,581.15 07/10101 56.44 54.96 5,581.51 08/20101 56.08 54.60 5,581.70 09/19/01 55.89 54.41 5,581.61 10102/01 55.98 54.50 5,581.83 11/08/01 55.76 54.28 5,582.17 12/03/01 55.42 53.94 5,582.21 01103/02 55.38 53.90 5,582.57 02/06102 55.02 53.54 5,583.12 03/26102 54.47 52.99 5,582.77 04/09/02 54.82 53.34 5,583.21 05/23/02 54.38 52.90 5,582.94 06105/02 54.65 53.17 5,582.71 07/08/02 54.88 53.40 5,583.67 08/23/02 53.92 52.44 5,583.82 09/11102 53.77 52.29 5,584.01 10/23/02 53.58 52.10 5,583.88 11122/02 53.71 52.23 5,583.81 12/03/02 53.78 52.30 5,584.28 01109/03 53.31 51.83 5,584.41 02/12/03 53.18 51.70 5,584.68 03/26103 52.91 51.43 5,584.49 04/02/03 53.10 51.62 5,584.51 05/01103 53.08 51.60 5,583.59 06109/03 54.00 52.52 5,582.96 07/07/03 54.63 53.15 5,582.98 08/04/03 54.61 53.13 5,582.57 09/11103 55.02 53.54 5,582.25 10102/03 55.34 53.86 5,582.09 11107/03 55.50 54.02 5,582.48 12/03/03 55.11 53.63 5,583.69 01115/04 53.90 52.42 5,583.89 02/10104 53.70 52.22 5,584.30 03/28/04 53.29 51.81 5,584.59 04/12/04 53.00 51.52 5,584.87 05/13/04 52.72 51.24 5,584.96 06/18/04 52.63 51.15 5,585.50 07/28/04 52.09 50.61 5,584.81 08/30104 52.78 51.30 5,584.40 09/16104 53.19 51.71 5,583.91 10/11104 53.68 52.20 5,583.39 11/16/04 54.20 52.72 Water Levels and Data over Time White Mesa Mill -Well TW 4-9 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,636.11 5,637.59 1.48 121.33 5,583.54 12/22/04 54.05 52.57 5,583.34 01118/05 54.25 52.77 5,583.66 02/28/05 53.93 52.45 5,583.87 03/15/05 53.72 52.24 5,584.74 04/26105 52.85 51.37 5,585.26 05/24/05 52.33 50.85 5,585.06 06/30105 52.53 51.05 5,584.67 07/29105 52.92 51.44 5,584.75 09/12/05 52.84 51.36 5,584.51 12/07/05 53.08 51.60 5,585.74 03/08/06 51.85 50.37 5,584.74 06113/06 52.85 51.37 5,584.26 07118/06 53.33 51.85 5,584.21 11107/06 53.38 51.90 5,584.67 02/27/07 52.92 51.44 5,584.06 05/02/07 53.53 52.05 5,585.33 08114/07 52.26 50.78 5,585.42 10110107 52.17 50.69 5,587.01 03/26108 50.58 49.10 5,585.44 06/24/08 52.15 50.67 5,585.23 08/26108 52.36 50.88 5,584.42 10/14/08 53.17 51.69 5,583.59 03/03/09 54.00 52.52 5,583.35 06/24/09 54.24 52.76 5,582.91 09/10109 54.68 53.20 5,583.43 12/11109 54.16 52.68 5,584.00 03111110 53.59 52.11 5,583.27 05111110 54.32 52.84 5,582.92 09/29/10 54.67 53.19 5,583.08 12/21110 54.51 53.03 5,582.63 02/28/11 54.96 53.48 5,583.62 06/21111 53.97 52.49 5,583.52 09/20111 54.07 52.59 5,583.91 12/21111 53.68 52.20 5,582.84 03/27112 54.75 53.27 5,582.84 06/28112 54.75 53.27 5,582.92 09/27112 54.67 53.19 Water Levels and Data over Time White Mesa Mill -Well TW 4-10 Total or Measuring Measured Water Land Point Depth to Total Depth Total Elevation Surface Elevation Length Of Date Of Water to Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,631.99 5,634.24 2.25 111 5,576.75 01103/02 57.49 55.24 5,576.92 02/06/02 57.32 55.07 5,577.43 03/26/02 56.81 54.56 5,577.22 04/09/02 57.02 54.77 5,577.80 05/23/02 56.44 54.19 5,577.47 06/05/02 56.77 54.52 5,577.55 07/08/02 56.69 54.44 5,578.l0 08/23/02 56.14 53.89 5,578.24 09111102 56.00 53.75 5,578.49 10/23/02 55.75 53.50 5,578.43 11122/02 55.81 53.56 5,578.43 12/03/02 55.81 53.56 5,578.66 01109/03 55.58 53.33 5,578.66 02112/03 55.58 53.33 5,578.78 03/26/03 55.46 53.21 5,578.90 04/02/03 55.34 53.09 5,578.83 05/01103 55.41 53.l6 5,578.05 06/09/03 56.19 53.94 5,577.38 07/07/03 56.86 54.61 5,577.15 08/04/03 57.09 54.84 5,576.76 09/11103 57.48 55.23 5,576.36 10102/03 57.88 55.63 5,576.05 11107/03 58.l9 55.94 5,576.20 12/03/03 58.04 55.79 5,577.43 01115/04 56.81 54.56 5,577.81 02110104 56.43 54.18 5,578.47 03/28/04 55.77 53.52 5,578.69 04112/04 55.55 53.30 5,578.93 05113/04 55.31 53.06 5,578.99 06118/04 55.25 53.00 5,579.l8 07/28/04 55.06 52.81 5,579.06 08/30104 55.18 52.93 5,578.78 09116/04 55.46 53.21 5,577.80 10111104 56.44 54.19 5,577.l3 11116/04 57.11 54.86 5,576.96 12/22/04 57.28 55.03 5,576.63 01118/05 57.61 55.36 5,576.82 02/28/05 57.42 55.17 5,576.86 03115/05 57.38 55.13 5,577.52 04/26/05 56.72 54.47 5,578.01 05/24/05 56.23 53.98 5,578.15 06/30105 56.09 53.84 5,577.90 07129/05 56.34 54.09 Water Levels and Data over Time White Mesa Mill -Well TW 4-10 Total or Measuring Measured Water Land Point Depth to Total Depth Total Elevation Surface Elevation Length Of Date Of Water to Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,631.99 5,634.24 2.25 111 5,578.02 09112/05 56.22 53.97 5,577.56 12/07/05 56.68 54.43 5,579.69 03/08/06 54.55 52.30 5,578.34 06/13/06 55.90 53.65 5,577.94 07118/06 56.30 54.05 5,578.01 11107/06 56.23 53.98 5578.43 02/27/07 55.81 53 .56 5,577.84 05/02/07 56.40 54.15 5,578.74 08114/07 55.50 53.25 5,579.04 10110107 55.20 52.95 5,580.69 03/26108 53.55 51.30 5,579.87 06/24/08 54.37 52.12 5,579.47 08/26108 54.77 52.52 5,578.87 10114/08 55.37 53.12 5,578.01 03110109 56.23 53.98 5,577.85 06/24/09 56.39 54.14 5,577.49 09110109 56.75 54.50 5,577.98 12111109 56.26 54.01 5,578.38 03111110 55.86 53.61 5,578.16 05111110 56.08 53.83 5,577.85 09/29110 56.39 54.14 5,577.28 12/21110 56.96 54.71 5,577.14 02/28111 57.1 54.85 5,578.09 06/21111 56.15 53.90 5,578.24 09/20111 56 53.75 5,578.74 12/21111 55.5 53.25 5,577.89 03/27112 56.35 54.10 5,577.90 06/28/12 56.34 54.09 5,578.29 09/27/12 55.95 53.70 Water Levels and Data over Time White Mesa Mill -Well TW 4-11 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,621.92 5,623.62 1.70 100 5,548.32 01103/02 75.30 73.60 5,548.73 02/06102 74.89 73.19 5,549.03 03/26102 74.59 72.89 5,548.84 04/09/02 74.78 73.08 5,549.30 05/23/02 74.32 72.62 5,549.01 06105/02 74.61 72.91 5,549.22 07/08/02 74.40 72.70 5,549.44 08/23/02 74.18 72.48 5,549.57 09111102 74.05 72.35 5,549.64 10/23/02 73.98 72.28 5,549.58 11122/02 74.04 72.34 5,549.62 12/03/02 74.00 72.30 5,549.85 01109/03 73.77 72.07 5,549.91 02112/03 73.71 72.01 5,550.15 03/26103 73.47 71.77 5,550.01 04/02/03 73.61 71.91 5,550.31 05/01103 73.31 71.61 5,550.44 06109/03 73.18 71.48 5,550.33 07/07/03 73.29 71.59 5,550.35 08/04/03 73.27 71.57 5,550.44 09111103 73.18 71.48 5,550.47 10102/03 73.15 71.45 5,550.60 11107/03 73.02 71.32 5,550.60 12/03/03 73.02 71.32 5,550.94 01115/04 72.68 70.98 5,551.00 02110104 72.62 70.92 5,550.34 03/28/04 73.28 71.58 5,551.54 04112/04 72.08 70.38 5,551.89 05/13/04 71.73 70.03 5,551.94 06118/04 71.68 69.98 5,552.49 07/28/04 71.13 69.43 5,552.74 08/30104 70.88 69.18 5,553.01 09116104 70.61 68.91 5,553.11 10111104 70.51 68.81 5,553.19 11116/04 70.43 68.73 5,553.53 12/22/04 70.09 68.39 5,553.31 01118/05 70.31 68.61 5,553.84 02/28/05 69.78 68.08 5,554.04 03115/05 69.58 67.88 5,554.23 04/26105 69.39 67.69 5,553.87 05/24/05 69.75 68.05 5,554.46 06/30105 69.16 67.46 5,554.57 07/29/05 69.05 67.35 Water Levels and Data over Time White Mesa Mill -Well TW 4-11 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,621.92 5,623.62 1.70 100 5,553.86 09112/05 69.76 68.06 5,555.30 12/07/05 68.32 66.62 5,556.20 03/08/06 67.42 65.72 5,556.48 06114/06 67.14 65.44 5,556.37 07118/06 67.25 65.55 5,556.94 11107/06 66.68 64.98 5557.92 02/27/07 65.70 64 5,557.84 05/02/07 65.78 64.08 5,558.02 08115/07 65.60 63.90 5,557.l3 10110107 66.49 64.79 5,569.74 03/26108 53.88 52.18 5,561.01 06/24/08 62.61 60.91 5,562.07 08/26108 61.55 59.85 5,562.47 10114/08 61.15 59.45 5,563.80 03110109 59.82 58.12 5,564.27 06/24/09 59.35 57.65 5,564.32 09110109 59.30 57.60 5,564.70 12111109 58.92 57.22 5,565.14 03111110 58.48 56.78 5,565.61 05111110 58.01 56.31 5,565.67 09/29110 57.95 56.25 5,565.62 12/21110 58.00 56.30 5,565.42 02/28111 58.20 56.50 5,566.01 06/21111 57.61 55.91 5,566.03 09/20111 57.59 55.89 5,566.63 12/21111 56.99 55.29 5,565.81 03/27112 57.81 56.11 5,565.82 06/28112 57.80 56.10 5,566.66 09/27112 56.96 55.26 Water Levels and Data over Time White Mesa Mill -Well TW 4-12 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,622.38 5,624.23 1.85 101.5 5,580.91 08/23/02 43.32 41.47 5,581.54 09111102 42.69 40.84 5,581.33 10123/02 42.90 41.05 5,581.47 11122/02 42.76 40.91 5,581.55 12/03/02 42.68 40.83 5,582.58 01109103 41.65 39.80 5,582.47 02112/03 41.76 39.91 5,582.71 03/26/03 41.52 39.67 5,582.11 04/02/03 42.12 40.27 5,582.92 05/01103 41.31 39.46 5,583.13 06/09103 41.10 39.25 5,583.21 07/07/03 41.02 39.17 5,583.31 08/04/03 40.92 39.07 5,583.55 09111103 40.68 38.83 5,583.72 10102/03 40.51 38.66 5,583.77 11107/03 40.46 38.61 5,584.01 12/03/03 40.22 38.37 5,584.37 01115/04 39.86 38.01 5,584.39 02110104 39.84 37.99 5,584.51 03/28/04 39.72 37.87 5,584.90 04112/04 39.33 37.48 5,584.88 05113/04 39.35 37.50 5,584.93 06118/04 39.30 37.45 5,585.36 07128/04 38.87 37.02 5,585.38 08/30104 38.85 37.00 5,585.49 09116/04 38.74 36.89 5,585.85 10111104 38.38 36.53 5,585.91 11116/04 38.32 36.47 5,586.35 12/22/04 37.88 36.03 5,586.14 01118/05 38.09 36.24 5,586.56 02/28/05 37.67 35.82 5,586.95 03115/05 37.28 35.43 5,587.20 04/26/05 37.03 35.18 5,587.35 05/24/05 36.88 35.03 5,587.58 06/30105 36.65 34.80 5,587.58 07/29105 36.65 34.80 5,587.94 09112/05 36.29 34.44 5,588.43 12/07/05 35.80 33.95 5,588.92 03/08/06 35.31 33.46 5,588.34 06/13/06 35.89 34.04 5,588.33 07118/06 35.90 34.05 5,584.70 11107/06 39.53 37.68 5588.85 02/27/07 35.38 33.53 Water Levels and Data over Time White Mesa Mill -Well TW 4-12 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,622.38 5,624.23 1.85 101.5 5,588.53 05102/07 35.70 33.85 5,586.49 08114/07 37.74 35.89 5,586.68 10110107 37.55 35.70 5,587.76 03/26/08 36.47 34.62 5,587.59 06/24/08 36.64 34.79 5,587.35 08/26/08 36.88 35.03 5,586.84 10114/08 37.39 35.54 5,586.17 03/03/09 38.06 36.21 5,585.74 06/24/09 38.49 36.64 5,585.54 09110109 38.69 36.84 5,585.77 12111109 38.46 36.61 5,585.88 03111110 38.35 36.50 5,586.35 05/11110 37.88 36.03 5,585.68 09/29110 38.55 36.70 5,585.09 12/21110 39.14 37.29 5,584.65 02/28111 39.58 37.73 5,584.76 06/21111 39.47 37.62 5,584.32 09/20111 39.91 38.06 5,584.22 12/21111 40.01 38.16 5,577.07 03 /27112 47.16 45.31 5,577.05 06/28112 47.18 45.33 5,583.14 09/27112 41.09 39.24 Water Levels and Data over Time White Mesa Mill -Well TW 4-13 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,618.09 5,619.94 1.85 102.5 5,529.66 08/23/02 90.28 88.43 5,530.66 09111102 89.28 87.43 5,529.10 10/23/02 90.84 88.99 5,530.58 11122/02 89.36 87.51 5,530.61 12/03/02 89.33 87.48 5,529.74 01109/03 90.20 88.35 5,531.03 02112/03 88.91 87.06 5,531.82 03/26/03 88.12 86.27 5,524.63 04/02/03 95.31 93.46 5,531.54 05/01103 88.40 86.55 5,538.46 06/09/03 81.48 79.63 5,539.38 07/07/03 80.56 78.71 5,540.72 08/04/03 79.22 77.37 5,541.25 09111103 78.69 76.84 5,541.34 10102/03 78.60 76.75 5,541.69 11107/03 78.25 76.40 5,541.91 12/03/03 78.03 76.18 5,542.44 01115/04 77.50 75.65 5,542.47 02110104 77.47 75.62 5,542.84 03/28/04 77.10 75.25 5,543.08 04112/04 76.86 75.01 5,543.34 05/13/04 76.60 74.75 5,543.40 06118/04 76.54 74.69 5,544.06 07/28/04 75.88 74.03 5,544.61 08/30104 75.33 73.48 5,545.23 09/16/04 74.71 72.86 5,546.20 10/11104 73.74 71.89 5,547.43 11116/04 72.51 70.66 5,548.96 12/22/04 70.98 69.13 5,549.02 01118/05 70.92 69.07 5,550.66 02/28/05 69.28 67.43 5,551.26 03115/05 68.68 66.83 5,552.23 04/26/05 67.71 65.86 5,552.87 05/24/05 67.07 65.22 5,553.42 06/30105 66.52 64.67 5,554.00 07/29/05 65.94 64.09 5,555.21 09112/05 64.73 62.88 5,558.13 12/07/05 61.81 59.96 5,562.93 03/08/06 57.01 55.16 5,564.39 06/13/06 55.55 53.70 5,562.09 07118/06 57.85 56.00 5,565.49 11107/06 54.45 52.60 5571.08 02/27/07 48.86 47.01 Water Levels and Data over Time White Mesa Mill -Well TW 4-13 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,618.09 5,619.94 1.85 102.5 5,570.63 05/02/07 49.31 47.46 5,565.24 08/14/07 54.70 52.85 5,565.83 10110107 54.11 52.26 5,569.29 03/26108 50.65 48.80 5,570.00 06124/08 49.94 48.09 5,570.41 08/26108 49.53 47.68 5,570.64 10114/08 49.30 47.45 5,570.43 03/03/09 49.51 47.66 5,570.56 06/24/09 49.38 47.53 5,570.42 09/10109 49.52 47.67 5,571.15 12/11109 48.79 46.94 5,572.01 03111110 47.93 46.08 5,572.88 05111110 47.06 45.21 5,573.17 09/29110 46.77 44.92 5,573.14 12/21110 46.80 44.95 5,573.10 02/28111 46.84 44.99 5,573.75 06/21111 46.19 44.34 5,573.63 09/20111 46.31 44.46 5,573.94 12/21111 46.00 44.15 5,572.79 03/27112 47.15 45.30 5,572.77 06/28/12 47.17 45.32 5,573.04 09/27/12 46.90 45.05 Water Levels and Data over Time White Mesa Mill -Well TW 4-14 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,610.92 5,612.77 1.85 93 5,518.90 08/23/02 93.87 92.02 5,519.28 09111102 93.49 91.64 5,519.95 10/23/02 92.82 90.97 5,520.32 11122/02 92.45 90.60 5,520.42 12/03/02 92.35 90.50 5,520.70 01109103 92.07 90.22 5,520.89 02112/03 91.88 90.03 5,521.12 03/26103 91.65 89.80 5,521.12 04/02/03 91.65 89.80 5,521.24 05/01103 91.53 89.68 5,521.34 06109103 91.43 89.58 5,521.36 07/07/03 91.41 89.56 5,521.35 08/04/03 91.42 89.57 5,521.30 09111103 91.47 89.62 5,521.35 10102/03 91.42 89.57 5,521.36 11107/03 91.41 89.56 5,521.16 12/03/03 91.61 89.76 5,521.29 01115/04 91.48 89.63 5,521.36 02110104 91.41 89.56 5,521.46 03/28/04 91.31 89.46 5,521.54 04112/04 91.23 89.38 5,521.59 05/13/04 91.18 89.33 5,521.69 06/18/04 91.08 89.23 5,521.71 07/28/04 91.06 89.21 5,521.76 08/30104 91.01 89.16 5,521.77 09116104 91.00 89.15 5,521.79 10111104 90.98 89.13 5,521.80 11116104 90.97 89.12 5,521.82 12/22/04 90.95 89.10 5,521.82 01118/05 90.95 89.10 5,521.86 02/28/05 90.91 89.06 5,521.85 03115/05 90.92 89.07 5,521.91 04/26105 90.86 89.01 5,521.93 05/24/05 90.84 88.99 5,521.94 06/30105 90.83 88.98 5,521.84 07/29105 90.93 89.08 5,521.99 09112/05 90.78 88.93 5,522.04 12/07/05 90.73 88.88 5,522.05 03/08/06 90.72 88.87 5,522.27 06113/06 90.50 88.65 5,521.92 07118/06 90.85 89.00 5,520.17 11107/06 92:60 90.75 5522.24 02/27/07 90.53 88.68 Water Levels and Data over Time White Mesa Mill -Well TW 4-14 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,610.92 5,612.77 1.85 93 5,522.47 05/02/07 90.30 88.45 5,520.74 08114/07 92.03 90.18 5,518.13 10110107 94.64 92.79 5,522.85 03/26/08 89.92 88.07 5,522.91 06/24/08 89.86 88.01 5,523.01 08/26/08 89.76 87.91 5,522.96 10114/08 89.81 87.96 5,523.20 03/03/09 89.57 87.72 5,523.33 06/24/09 89.44 87.59 5,523.47 09110109 89.30 87.45 5,523.54 12/11109 89.23 87.38 5,522.98 03/1111 0 89.79 87.94 5,524.01 05111110 88.76 86.91 5,524.37 09/29110 88.40 86.55 5,524.62 12/21110 88.15 86.30 5,524.78 02/28111 87.99 86.14 5,525.23 06/21111 87.54 85.69 5,525.45 09/20111 87.32 85.47 5,525.72 12/21111 87.05 85.20 5,525.88 03/27112 86.89 85.04 5,525.97 06/28112 86.80 84.95 5,526.32 09/27112 86.45 84.60 I. Water Levels and Data over Time White Mesa Mill-Well MW-26 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,624.15 5,625.45 1.30 121.33 5,574.75 08/23/02 50.70 49.40 5,574.97 09/11102 50.48 49.18 5,575.10 10/23/02 50.35 49.05 5,574.99 11122/02 50.46 49.16 5,575.28 12/03/02 50.17 48.87 5,575.41 01109/03 50.04 48.74 5,575.43 02/12/03 50.02 48.72 5,575.63 03/26/03 49.82 48.52 5,575.91 04/02/03 49.54 48.24 5,575.81 05/01103 49.64 48.34 5,572.36 06/09/03 53.09 51.79 5,570.70 07/07/03 54.75 53.45 5,570.29 08/04/03 55.16 53.86 5,560.94 09/11103 64.51 63.21 5,560.63 10102/03 64.82 63.52 5,560.56 11107/03 64.89 63.59 5,564.77 12/03/03 60.68 59.38 5,570.89 01115/04 54.56 53.26 5,572.55 02/10104 52.90 51.60 5,574.25 03/28/04 51.20 49.90 5,574.77 04/12/04 50.68 49.38 5,575.53 05/13/04 49.92 48.62 5,575.59 06/18/04 49.86 48.56 5,576.82 07/28/04 48.63 47.33 5,527.47 09/16/04 97.98 96.68 5,553.97 11/16/04 71.48 70.18 5,562.33 12/22/04 63.12 61.82 5,550.00 01118/05 75.45 74.15 5,560.02 04/26/05 65.43 64.13 5,546.11 05/24/05 79.34 78.04 5,556.71 06/30105 68.74 67.44 5,554.95 07/29/05 70.50 69.20 5,555.48 09/12/05 69.97 68.67 5,551.09 12/07/05 74.36 73.06 5,552.85 03/08/06 72.60 71.30 5,554.30 06/13/06 71.15 69.85 5,554.87 07/18/06 70.58 69.28 5,550.88 11107/06 74.57 73.27 5558.77 02/27/07 66.68 65.38 5,548.54 05/02/07 76.91 75.61 5,551.33 10/10107 74.12 72.82 5,545.56 03/26/08 79.89 78.59 5,545.56 06/25/08 79.89 78.59 Water Levels and Data over Time White Mesa Mill-Well MW-26 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,624.15 5,625.45 1.30 121.33 5,545.82 08/26/08 79.63 78.33 5,545.64 10114/08 79.81 78.51 5,544.45 03/03/09 81.00 79.70 5,545.32 06/24/09 80.13 78.83 5,544.61 09110109 80.84 79.54 5,549.33 12111109 76.12 74.82 5,543.78 03111110 81.67 80.37 5,545.61 05111110 79.84 78.54 5,547.43 09/29110 78.02 76.72 5,544.14 12/21110 81.31 80.01 5,546.77 02/28111 78.68 77.38 5,537.60 06/21111 87.85 86.55 5,551.46 09/20111 73.99 72.69 5,549.12 12/21111 76.33 75.03 5,557.30 03/27112 68.15 66.85 5,557.38 06/28112 68.07 66.77 5,550.86 09/27112 74.59 73.29 Water Levels and Data over Time White Mesa Mill -Well TW 4-16 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,622.19 5,624.02 1.83 142 5,562.91 08/23/02 61.11 59.28 5,563.45 09111102 60.57 58.74 5,563.75 10/23/02 60.27 58.44 5,563.68 11122/02 60.34 58.51 5,563.68 12/03/02 60.34 58.51 5,564.16 01109/03 59.86 58.03 5,564.25 02112/03 59.77 57.94 5,564.53 03/26/03 59.49 57.66 5,564.46 04/02/03 59.56 57.73 5,564.79 05/01103 59.23 57.40 5,564.31 06/09/03 59.71 57.88 5,563.29 07/07/03 60.73 58.90 5,562.76 08/04/03 61.26 59.43 5,561.73 09111103 62.29 60.46 5,561.04 10102/03 62.98 61.15 5,560.39 11/07/03 63.63 61.80 5,559.79 12/03/03 64.23 62.40 5,561.02 01115/04 63.00 61.17 5,561.75 02110104 62.27 60.44 5,562.98 03/28/04 61.04 59.21 5,563.29 04112/04 60.73 58.90 5,564.03 05113/04 59.99 58.16 5,564.09 06118/04 59.93 58.10 5,565.08 07/28/04 58.94 57.11 5,564.56 08/30104 59.46 57.63 5,563.55 09116/04 60.47 58.64 5,561.79 10111104 62.23 60.40 5,560.38 11116/04 63.64 61.81 5,559.71 12/22/04 64.31 62.48 5,559.14 01118/05 64.88 63.05 5,558.65 02/28/05 65.37 63.54 5,558.54 03115/05 65.48 63.65 5,558.22 04/26/05 65.80 63.97 5,558.54 05/24/05 65.48 63.65 5,559.24 06/30105 64.78 62.95 5,559.38 07/29/05 64.64 62.81 5,559.23 09112/05 64.79 62.96 5,557.67 12/07/05 66.35 64.52 5,557.92 03/08/06 66.10 64.27 5,558.47 06113/06 65.55 63.72 5,558.42 07118/06 65.60 63.77 5,558.09 11/07/06 65.93 64.10 5557.34 02/27/07 66.68 64.85 Water Levels and Data over Time White Mesa Mill-Well TW4-16 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,622.19 5,624.02 1.83 142 5,547.11 05/02/07 76.91 75 .08 5,558.52 08114/07 65.50 63.67 5,559.02 10110107 65.00 63.17 5,561.04 03/26108 62.98 61.15 5,560.06 06/24/08 63.96 62.13 5,559.32 08/26108 64.70 62.87 5,558.89 10114/08 65.13 63.30 5,558.40 03/03/09 65.62 63.79 5,558.32 06/24/09 65.70 63.87 5,558.03 09/10109 65.99 64.16 5,558.81 12/11109 65.21 63.38 5,559.80 03111110 64.22 62.39 5,559.85 05/11110 64.17 62.34 5,560.54 09/29110 63.48 61.65 5,558.65 12/21110 65.37 63 .54 5,559.26 02/28111 64.76 62.93 5,560.48 06/21111 63.54 61.71 5,561.52 09/20111 62.50 60.67 5,562.95 12/21111 61.07 59.24 5,563.76 03/27112 60.26 58.43 5,563.90 06/28112 60.12 58.29 5,564.65 09/27/12 59.37 57.54 Water Levels and Data over Time White Mesa Mill-Well MW-32 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,623.41 5,625.24 1.83 130.6 5,542.17 08/23/02 83.07 81.24 5,542.39 09111102 82.85 81.02 5,542.61 10/23/02 82.63 80.80 5,542.49 11/22/02 82.75 80.92 5,542.82 12/03/02 82.42 80.59 5,543.03 01109103 82.21 80.38 5,543.04 02112/03 82.20 80.37 5,543.41 03/26103 81.83 80.00 5,543.69 04/02/03 81.55 79.72 5,543.77 05/01103 81.47 79.64 5,544.01 06109103 81.23 79.40 5,544.05 07/07/03 81.19 79.36 5,543.99 08/04/03 81.25 79.42 5,544.17 09111103 81.07 79.24 5,544.06 10102/03 81.18 79.35 5,544.03 11107/03 81.21 79.38 5,543.94 12/03/03 81.30 79.47 5,543.98 01115/04 81.26 79.43 5,543.85 02110104 81.39 79.56 5,544.05 03/28/04 81.19 79.36 5,544.33 04112/04 80.91 79.08 5,544.55 05/13/04 80.69 78.86 5,544.59 06118/04 80.65 78.82 5,545.08 07/28/04 80.16 78.33 5,545.26 08/30104 79.98 78.15 5,545.48 09116104 79.76 77.93 5,545.61 10111104 79.63 77.80 5,545.46 11116/04 79.78 77.95 5,545.66 12/22/04 79.58 77.75 5,545.33 01118/05 79.91 78.08 5,545.51 02/28/05 79.73 77.90 5,545.57 03115/05 79.67 77.84 5,545.46 04/26105 79.78 77.95 5,545.45 05/24/05 79.79 77.96 5,545.33 06/30105 79.91 78.08 5,545.16 07/29105 80.08 78.25 5,545.54 09112/05 79.70 77.87 5,545.77 12/07/05 79.47 77.64 5,546.09 03/08/06 79.15 77.32 5,545.94 06113/06 79.30 77.47 5,545.94 07118/06 79.30 77.47 5,546.24 11107/06 79.00 77.17 5546.81 02/27/07 78.43 76.6 Water Levels and Data over Time White Mesa Mill-Well MW-32 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,623.41 5,625.24 l.83 130.6 5546.56 05/02/07 78.68 76.85 5546.81 08/15/07 78.43 76.6 5546.96 10/10107 78.28 76.45 5547.9 03/26/08 77.34 75.51 5548.08 06/25/08 77.16 75.33 5548.42 08/26/08 76.82 74.99 5548.05 10/14/08 77.19 75.36 5548.29 03/03/09 76.95 75.12 5548.09 06/24/09 77.15 75.32 5547.79 09/10109 77.45 75.62 5548.09 12/11/09 77.15 75.32 5,548.50 03/11/10 76.74 74.91 5,548.89 05111/10 76.35 74.52 5,548.83 09/29110 76.41 74.58 5,548.97 12/21110 76.27 74.44 5,548.68 02/28/11 76.56 74.73 5,549.33 06/21111 75.91 74.08 5,549.l9 09/20111 76.05 74.22 5,550.06 12/21111 75.l8 73.35 5,550.31 03/27/12 74.93 73.10 5,550.32 06/28/12 74.92 73.09 5,550.88 09/27/12 74.36 72.53 Water Levels and Data over Time White Mesa Mill -Well TW 4-18 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,639.13 5,641.28 2.15 137.5 5,585.13 08/23/02 56.15 54.00 5,585.41 09/11/02 55.87 53.72 5,585.47 10/23/02 55.81 53.66 5,585.40 11122/02 55.88 53.73 5,585.68 12/03/02 55.60 53.45 5,585.90 01109/03 55.38 53.23 5,590.79 02/12/03 50.49 48.34 5,586.18 03/26103 55.10 52.95 5,586.36 04/02/03 54.92 52.77 5,586.24 05/01103 55.04 52.89 5,584.93 06109/03 56.35 54.20 5,584.46 07/07/03 56.82 54.67 5,584.55 08/04/03 56.73 54.58 5,584.01 09/11/03 57.27 55.12 5,583.67 10102/03 57.61 55.46 5,583.50 11107/03 57.78 55.63 5,584.08 12/03/03 57.20 55.05 5,585.45 01115/04 55.83 53.68 5,585.66 02/10104 55.62 53.47 5,586.13 03/28/04 55.15 53.00 5,586.39 04/12/04 54.89 52.74 5,586.66 05/13/04 54.62 52.47 5,586.77 06/18/04 54.51 52.36 5,587.35 07/28/04 53.93 51.78 5,586.34 08/30104 54.94 52.79 5,585.85 09/16104 55.43 53.28 5,585.22 10/11104 56.06 53.91 5,584.70 11/16/04 56.58 54.43 5,584.81 12/22/04 56.47 54.32 5,584.68 01118/05 56.60 54.45 5,585.02 02/28/05 56.26 54.11 5,585.25 03/15/05 56.03 53.88 5,586.31 04/26105 54.97 52.82 5,586.97 05/24/05 54.31 52.16 5,586.58 06/30105 54.70 52.55 5,586.10 07/29/05 55.18 53.03 5,586.05 09/12/05 55.23 53.08 5,585.86 12/07/05 55.42 53.27 5,587.13 03/08/06 54.15 52.00 5,585.93 06/13/06 55.35 53.20 5,585.40 07/18/06 55.88 53.73 5,585.38 11107/06 55.90 53.75 5585.83 02/27/07 55.45 53.30 Water Levels and Data over Time White Mesa Mill -Well TW 4-18 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,639.13 5,641.28 2.15 137.5 5585.15 05/02/07 56.13 53.98 5586.47 06/24/08 54.81 52.66 5586.3 08/26108 54.98 52.83 5585.21 10114/08 56.07 53.92 5584.47 03/03/09 56.81 54.66 5584.35 06/24/09 56.93 54.78 5583.88 09110109 57.4 55.25 5584.43 12111109 56.85 54.70 5,585.26 03111110 56.02 53.87 5,584.17 05111110 57.11 54.96 5,583.61 09/29110 57.67 55.52 5,604.29 12/21110 36.99 34.84 5,583.56 02/28111 57.72 55.57 5,584.73 06/21111 56.55 54.40 5,584.71 09/20111 56.57 54.42 5,585.03 12/21111 56.25 54.10 5,584.63 03/27112 56.65 54.50 5,584.67 06/28/12 56.61 54.46 5,583.98 09/27112 57.30 55.15 Water Levels and Data over Time White Mesa Mill -Well TW 4-19 Total or Measuring Measured Water Land Point Depth to Total Depth Elevation Surface Elevation Length Of Date Of Water to Water Total Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,629.53 5,631.39 1.86 121.33 5,581.88 08/23/02 49.51 47.65 5,582.14 09/11102 49.25 47.39 5,582.06 10/23/02 49.33 47.47 5,582.07 11122/02 49.32 47.46 5,582.l6 12/03/02 49.23 47.37 5,582.28 01109/03 49.l1 47.25 5,582.29 02/21103 49.10 47.24 5,582.74 03/26/03 48.65 46.79 5,582.82 04/02/03 48.57 46.71 5,548.47 05/01103 82.92 81.06 5,564.76 06/09/03 66.63 64.77 5,562.53 07/07/03 68.86 67.00 5,564.l0 08/04/03 67.29 65.43 5,566.01 08/30104 65.38 63.52 5,555.16 09116/04 76.23 74.37 5,549.80 10111104 81.59 79.73 5,546.04 11116/04 85.35 83.49 5,547.34 12/22/04 84.05 82.19 5,548.77 01118/05 82.62 80.76 5,551.18 02/28/05 80.21 78.35 5,556.81 03115/05 74.58 72.72 5,562.63 04/26/05 68.76 66.90 5,573.42 05/24/05 57.97 56.11 5,552.94 07/29/05 78.45 76.59 5,554.00 09112/05 77.39 75.53 5,555.98 12/07/05 75.41 73.55 5,552.00 03/08/06 79.39 77.53 5,545.74 06113/06 85.65 83.79 5,544.06 07118/06 87.33 85.47 5,548.81 11107/06 82.58 80.72 5543.59 02/27/07 87.80 85.94 5544.55 05/02/07 86.84 84.98 5558.97 08/15/07 72.42 70.56 5559.73 10/10107 71.66 69.8 5569.26 03/26/08 62.13 60.27 5535.47 06/25/08 95.92 94.06 5541.41 08/26/08 89.98 88.12 5558.45 10114/08 72.94 71.08 5536.9 03/03/09 94.49 92.63 5547.76 06/24/09 83.63 81.77 5561.48 09110109 69.91 68.05 5548.l4 12111109 83.25 81.39 5,570.58 03111110 60.81 58.95 Water Levels and Data over Time White Mesa Mill -Well TW 4-19 Total or Measuring Measured Water Land Point Depth to Total Depth Elevation Surface Elevation Length Of Date Of Water to Water Total Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,629.53 5,631.39 1.86 121.33 5,561.35 05111110 70.04 68.18 5,535.26 09/29110 96.13 94.27 5,568.40 12/21110 62.99 61.13 5,550.36 02/28111 81.03 79.17 5,570.41 06/21111 60.98 59.12 5,567.84 09/20111 63.55 61.69 5,571.32 12/21111 60.07 58.21 5,572.40 03/27112 58.99 57.13 5,572.39 06/28112 59.00 57.14 5,571.40 09/27112 59.99 58.13 Water Levels and Data over Time White Mesa Mill -Well TW 4-20 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,628.52 5,629.53 1.01 106.0 5,565.70 07/29/05 63.83 62.82 5,546.53 08/30105 83.00 81.99 5,540.29 09112/05 89.24 88.23 5,541.17 12/07/05 88.36 87.35 5,540.33 03/08/06 89.20 88.19 5,530.43 06/13/06 99.10 98.09 5,569.13 07/18/06 60.40 59.39 5,547.95 11107/06 81.58 80.57 5,549.25 02/27/07 80.28 79.27 5,550.58 05/02/07 78.95 77.94 5,563.60 08114/07 65.93 64.92 5,555.85 10/10107 73.68 72.67 5,569.10 03/26/08 60.43 59.42 5,560.00 06/25/08 69.53 68.52 5,539.64 08/26/08 89.89 88.88 5,539.51 10114/08 90.02 89.01 5,553.00 03/03/09 76.53 75.52 5,534.18 06/24/09 95.35 94.34 5,558.39 09110109 71.14 70.13 5,560.99 12/11109 68.54 67.53 5,564.09 03111110 65.44 64.43 5,564.22 05111110 65.31 64.30 5,560.33 09/29110 69.20 68.19 5,561.35 12/21110 68.18 67.17 5,560.18 02/28/11 69.35 68.34 5,576.23 06/21111 53.30 52.29 5,548.50 09/20111 81.03 80.02 5,558.58 12/21111 70.95 69.94 5,567.73 03/27112 61.80 60.79 5,567.77 06/28112 61.76 60.75 5,569.58 09/27112 59.95 58.94 Water Levels and Data over Time White Mesa Mill -Well TW 4-21 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,638.20 5,639.35 l.15 120.92 5,582.98 07/29/05 56.37 55.22 5,583.43 08/30105 55.92 54.77 5,58l.87 09112/05 57.48 56.33 5,580.50 12/07/05 58.85 57.70 5,583.64 03/08/06 55.71 54.56 5,580.55 06/13/06 58.80 57.65 5,578.95 07/18/06 60.40 59.25 5,578.47 11107/06 60.88 59.73 5,579.53 02/27/07 59.82 58.67 5,578.07 05/02/07 6l.28 60.13 5,583.41 08/15/07 55.94 54.79 5,583.45 10110107 55.90 54.75 5,586.47 03/26108 52.88 5l.73 5,579.16 06/24/08 60.19 59.04 5,579.92 08/26108 59.43 58.28 5,577.37 10/14/08 6l.98 60.83 5,578.00 03110109 6l.35 60.20 5,580.14 06/24/09 59.21 58.06 5,578.72 09/10109 60.63 59.48 5,579.99 12111109 59.36 58.21 5,582.81 03/11110 56.54 55.39 5,582.23 05111110 57.12 55.97 5,576.60 09/29/10 62.75 6l.60 5,58l.14 12/21110 58.21 57.06 5,579.53 02/28111 59.82 58.67 5,584.17 06/21111 55.18 54.03 5,584.80 09/20/11 54.55 53.40 5,585.68 12/21111 53.67 52.52 5,585.24 03/27112 54.11 52.96 5,585.26 06/28112 54.09 52.94 5,585.16 09/27112 54.19 53.04 Water Levels and Data over Time White Mesa Mill -Well TW 4-22 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,627.83 5,629.00 1.17 113.5 5,571.89 07/29/05 57.11 55.94 5,572.20 08/30105 56.80 55.63 5,572.08 09112/05 56.92 55.75 5,571.61 12/07/05 57.39 56.22 5,571.85 03/08/06 57.15 55.98 5,571.62 06113/06 57.38 56.21 5,571.42 07118/06 57.58 56.41 5,571.02 11107/06 57.98 56.81 5571.24 02/27/07 57.76 56.59 5,570.75 06/29/07 58.25 57.08 5,571.82 08114/07 57.18 56.01 5,571.99 10110107 57.01 55.84 5,573.05 03/26108 55.95 54.78 5,573.04 06/24/08 55.96 54.79 5,573.04 08/26108 55.96 54.79 5,573.02 10114/08 55.98 54.81 5,573.19 03/10109 55.81 54.64 5,573.32 06/24/09 55.68 54.51 5,573.17 09110109 55.83 54.66 5,573.52 12111109 55.48 54.31 5,573.88 03111110 55.12 53.95 5,574.29 05111110 54.71 53.54 5,574.88 09/29110 54.12 52.95 5,574.44 12/21110 54.56 53.39 5,574.49 02/28111 54.51 53.34 5,574.97 06/21111 54.03 52.86 5,575.06 09/20111 53.94 52.77 5,575.69 12/21111 53.31 52.14 5,575.61 03/27112 53.39 52.22 5,575.62 06/28112 53.38 52.21 5,575.90 09/27112 53.10 51.93 Water Levels and Data over Time White Mesa Mill -Well TW 4-23 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,605.77 5,607.37 1.60 113.5 5,538.89 09113/07 68.48 66.88 5,538.80 10110107 68.57 66.97 5,539.25 11130107 68.12 66.52 5,539.49 12111107 67.88 66.28 5,539.19 01108/08 68.18 66.58 5,539.44 02118/08 67.93 66.33 5,539.54 03/26/08 67.83 66.23 5,539.71 04/23/08 67.66 66.06 5539.48 05/30108 67.89 66.29 5,539.53 06/24/08 67.84 66.24 5,539.44 07116/08 67.93 66.33 5,539.68 08/26/08 67.69 66.09 5,541.18 09110108 66.19 64.59 5,539.57 10114/08 67.80 66.20 5,539.29 11126/08 68.08 66.48 5,539.55 12/29/08 67.82 66.22 5,540.15 01126/09 67.22 65.62 5,539.74 02/24/09 67.63 66.03 5,539.86 03/06/09 67.51 65.91 5,539.72 04/07/09 67.65 66.05 5,539.84 05/29/09 67.53 65.93 5,540.12 06/30109 67.25 65.65 5,540.12 07/31109 67.25 65.65 5,540.27 08/31109 67.10 65.50 5,540.13 09110109 67.24 65.64 5,540.64 12111109 66.73 65.13 5,541.15 03111110 66.22 64.62 5,541.61 05111110 65.76 64.16 5,541.47 09/29110 65.90 64.30 5,541.54 12/21110 65.83 64.23 5,541.54 02/28111 65.83 64.23 5,541.98 06/21111 65.39 63.79 5,541.90 09/20/11 65.47 63.87 5,542.58 12/21111 64.79 63.19 5,542.59 03/27112 64.78 63.18 5,542.61 06/28112 64.76 63.16 5,542.92 09/27112 64.45 62.85 Water Levels and Data over Time White Mesa Mill -Well TW 4-24 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,625.70 5,627.83 2.13 113.5 5,570.61 09113/07 57.22 55.09 5,570.53 10110107 57.30 55.17 5,571.16 11130107 56.67 54.54 5,571.30 12111107 56.53 54.40 5,571.03 01108/08 56.80 54.67 5,571.22 02118/08 56.61 54.48 5,571.43 03/26/08 56.40 54.27 5,571.68 04/23/08 56.15 54.02 5571.52 05/30108 56.31 54.18 5,571.34 06/24/08 56.49 54.36 5,571.28 07116/08 56.55 54.42 5,571.34 08/26/08 56.49 54.36 5,571.23 09110108 56.60 54.47 5,571.12 10114/08 56.71 54.58 5,570.95 11126/08 56.88 54.75 5,570.92 12/29/08 56.91 54.78 5,571.65 01126/09 56.18 54.05 5,571.31 02/24/09 56.52 54.39 5,571.37 03/06/09 56.46 54.33 5,571.21 04/07/09 56.62 54.49 5,571.23 05/29/09 56.60 54.47 5,571.42 06/30109 56.41 54.28 5,571.38 07/31109 56.45 54.32 5,571.48 08/31109 56.35 54.22 5,571.28 09110109 56.55 54.42 5,571.64 12111109 56.19 54.06 5,571.86 03111110 55.97 53.84 5,571.91 05111110 55.92 53.79 5,572.18 09/29110 55.65 53.52 5,571.86 12/21110 55.97 53.84 5,571.78 02/28111 56.05 53.92 5,572.40 06/21111 55.43 53.30 5,572.19 09/20111 55.64 53.51 5,573.02 12/21111 54.81 52.68 5,573.03 03/27112 54.80 52.67 5,573.02 06/28112 54.81 52.68 5,573.13 09/27112 54.70 52.57 Water Levels and Data over Time White Mesa Mill -Well TW 4-25 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,627.83 5,644.91 17.08 134.8 5,601.86 09113/07 43.05 25.97 5,601.89 10110107 43.02 25.94 5,602.57 11130107 42.34 25.26 5,602.82 12111107 42.09 25.01 5,601.94 01108/08 42.97 25.89 5,599.13 02118/08 45.78 28.70 5,597.11 03/26108 47.80 30.72 5,595.51 04/23/08 49.40 32.32 5594.42 05/30108 50.49 33.41 5,594.26 06/24/08 50.65 33.57 1 5,586.67 07116108 58.24 41.16 5,594.17 08/26108 50.74 33.66 5,594.23 09110108 50.68 33.60 5,594.12 10114/08 50.79 33.71 5,594.06 11126/08 50.85 33.77 5,594.87 12/29/08 50.04 32.96 5,595.89 01126109 49.02 31.94 5,596.27 02/24/09 48.64 31.56 5,596.47 03/06109 48.44 31.36 5,596.74 04/07/09 48.17 31.09 5,597.55 05/29/09 47.36 30.28 5,598.11 06/30109 46.80 29.72 5,598.22 07/31109 46.69 29.61 5,598.52 08/31109 46.39 29.31 5,598.49 09110109 46.42 29.34 5,599.48 12111109 45.43 28.35 5,599.75 03111110 45.16 28.08 5,599.63 05111110 45.28 28.20 5,598.68 09/29110 46.23 29.15 5,598.66 12/21110 46.25 29.17 5,598.18 02/28111 46.73 29.65 5,598.61 06/21111 46.30 29.22 5,598.08 09/20111 46.83 29.75 5,598.23 12/21111 46.68 29.60 5,597.41 03/27112 47.50 30.42 5,597.41 06/28112 47.50 30.42 5,595.60 09/27112 49.31 32.23 Water Levels and Data over Time White Mesa Mill -Well TW 4-26 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,599.98 5,601.68 1.70 86 5,536.90 06114110 64.78 63.08 5,536.95 09/29110 64.73 63.03 5,537.17 12/21110 64.51 62.81 5,537.16 02/28111 64.52 62.82 5,537.57 06/21111 64.11 62.41 5,537.59 09/20111 64.09 62.39 5,538.16 12/21111 63.52 61.82 5,538.18 03/27112 63.50 61.80 5538.23 06/28112 63.45 61.75 5,538.57 09/27112 63.11 61.41 Water Levels and Data over Time White Mesa Mill-Well TW4-27 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,606.19 5,607.94 1.75 96 5,517.78 12/21111 90.16 88.41 5,524.84 03/27112 83.10 81.35 5,524.93 06/28112 83.01 81.26 5,525.59 09/27112 82.35 80.60 TabH Laboratory Analytical Reports EI\ERGY LABORATORIES www.energyJab.com Analytical ExcsfiBfICB Sines 7952 Helena, MT 877-472-0111 • Billings, MT 800-135-4489 . Casper, WY 888-235-0515 ~iII~tte, Wy 866-686-7175 .. Rapid City, SD 888-672-1225 .. College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 LablD: C 12090222-003 Client Sample ID: MW-04_09042012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 41 5.0 1.5 1500 NO NO 118 148 140 129 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl o 1 0.5 1.0 o 50 1.0 1.0 80-120 S 70-130 S 80-120 S 80-120 Report Date: 09/25/12 Collection Date: 09/04/12 14:10 DateReceived: 09/07/12 Matrix: Aqueous MCL! QCl Method E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B Analysis Date 1 By 09/11/12 20:221 wc 09/10/12 11 :16 1 Ir 09/11/12 18:481 jk 09/13/12 16:341 jk 09/11/1218:481 jk 09/11/1218:481 jk 09/11/12 18 :48 1 jk 09/11/1218:481 jk 09/11/1218:481 jk 09/11/12 18:481 jk MCl -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 5 of 19 EN:RGY LABORATORIES www.energylab.com Analytical Exes/lanes Sines 79S1 Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/13/1207:17 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Lab ID: C12090481-012 Client Sample 10: TW4-01_09132012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dS Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 39 5 ND 1000 ND ND 111 102 111 93.0 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl D 1.0 D 100 1.0 1.0 SO-120 70-130 SO-120 SO-120 MCL! QCl Method E300.0 E353.2 SWS260B SWS260B SWS260B SWS260B SWS260B SWS260B SWS260B SWS260B MCl -Maximum contaminant level. Analysis Date 1 By 09/1S/12 01 :30 1 wc 09/17/1215:09/1r 09/26/1205:221 jk 09/26/12 16:441 jk 09/26/12 05:221 jk 09/26/12 05:221 jk 09/26/12 05:221 jk 09/26/12 05 :22 1 jk 09/26/12 05:221 jk 09/26/12 05:221 jk ND -Not detected at the reporting limit. Page 14 of 28 EI'.ERGY LABORATORIES www.energyJab.com Analytical ExCSUsncB Sines 1852 Helena, MT 811-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/13/12 07:30 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 LablD: C 12090481-0.13 Client Sample ID: TW4-02_09132012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 76 4 1.8 2900 NO NO 111 99.0 111 93.0 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl 0 2 0 1.0 0 100 1.0 1.0 80-120 70-130 80-120 80-120 MCL! QCl Method E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B MCl -Maximum contaminant level. Analysis Date / By 09/18/12 19:081 wc 09/17/1215:12/1r 09/26/12 05:581 jk 09/26/12 17:191 jk 09/26/1205:581 jk 09/26/12 05:581 jk 09/26/12 05:58 1 jk 09/26/12 05:581 jk 09/26/12 05:581 jk 09/26/12 05:581 jk NO -Not detected at the reporting limit. Page 15 of 28 EI\ERGY LABORATORIES www.energyJab.com Analytical UCSUBllCfJ Sincs 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: LablD: 3rd Quarter Chloroform Sampling 2012 C12081321-002 Client Sample ID: TW4-03_08292012 Analyses MAJOR IONS . Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 25 4.9 NO NO NO NO 108 122 126 116 0-Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/12/12 Collection Date: 08/29/1206:26 DateReceived: 08/31/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date / By o 0.5 1.0 1.0 1.0 1.0 80-120 70-130 E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B 09/06/12 20:061 wc 09/04/1213:00 fiji 09/04/12 16:551 jk 09/04/12 16:551 jk 09/04/1216:551 jk 09/04/12 16:551 jk 09/04/12 16:55 1 jk 09/04/12 16:55 1 jk S 80-120 SW8260B 09/04/12 16:55 1 jk 80-120 SW8260B 09/04/12 16:55 1 jk MCl -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 4 of 23 EI\ERGY LABORATORIES www.energylab.com Analytical ExcsJlBnctl Sincs '952 Helena, MT 877 -412-0711 • Billings, MT 800-735-4489 • Casper, Wi 888-235-0515 ~illette, WY 866-686-7115 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: LablD: 3rd Quarter Chloroform Sampling 2012 C12081321-001 Client Sample ID: TW4-03R_08282012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units NO mg/l NO mg/l NO ug/l NO ug/l NO ug/l NO ug/l 106 %REC 125 %REC 126 %REC 116 %REC S -Spike recovery outside of advisory limits. Report Date: 09/12/12 Collection Date: 08/28/12 07:32 DateReceived: 08/31/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By S 0.1 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B MCl -Maximum contaminant level. 09/06/12 19:491 wc 09/04/12 12:57 1 Ijl 09/07/12 16:361 jk 09/07/12 16:361 jk 09/07/1216:36/jk 09/07/1216:36/jk 09/07/12 16:361 jk 09/07/12 16:361 jk 09/07/12 16:361 jk 09/07/12 16:361 jk NO -Not detected at the reporting limit. Page 3 of 23 EN:RGY LASORATORIES www.energylab.com ( Analytical ExcsHtmCfJ Sincs 7952 )~ Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WV 888-235-0515 ~ille.ttll, WY 866-686-7175 II Rapid City, SD 888-672-1225 II College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 LablD: C 12090222-004 Client Sample ID: TW4-04_09042012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: T 0luene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 39 7.1 1.2 1600 ND ND 119 161 140 129 0-Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl D 0.2 1.0 D 50 1.0 1.0 80-120 S 70-130 S 80-120 S 80-120 Report Date: 09/25/12 Collection Date: 09/04/12 14:25 DateReceived: 09/07/12 Matrix: Aqueous MCL! QCl Method E300.0 E353.2 SW8260B SW8260B SW8260B . SW8260B SW8260B SW8260B SW8260B SW8260B Analysis Date 1 By 09/11/12 21 : 14 1 wc 09/10/12 11 :18 1 Ir 09/11/1219:231 jk 09/13/12 17:09 1 jk 09/11/1219:231 jk 09/11/1219:231 jk 09/11/12 19:231 jk 09/11/12 19:231 jk 09/11/12 19:231 jk 09/11/1219:23/jk MCl -Maximum contaminant level. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 6 of 19 00' www.energyt.b.com r---He~n •• MT817-412-0711 .Billings.MT 801-135-0\489 • Casper, WY 888-235-8515 -~ AnalyticalExcsUsncsSincs 1652 j Gillette, WY 866-686-7175 -Rapid City, SD 888-672-1225 -College Station, IX 888-&90-2218 EI\ERGY LABORATORIES LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/11/1207:35 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Lab ID: C 12090481-005 Client Sample ID: TW4-05_09112012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 37 8.1 ND 12 ND ND 116 138 130 112 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier RL D 1 0.5 1.0 1.0 1.0 1.0 80-120 S 70-130 S 80-120 80-120 MCL! QCL Method E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B MCl -Maximum contaminant level. Analysis Date 1 By 09/17/1223:281 wc 09/17/1214:39/1r 09/24/12 02:431 jk 09/24/12 02:431 jk 09/24/1202:43/ jk 09/24/12 02:43/ jk 09/24/12 02:43 1 jk 09/24/12 02:43 / jk 09/24/12 02:43 / jk 09/24/12 02:43/ jk ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 70f28 EN:RGY LABORAT ORIES www.energylab.com Analytical ExcsHsocs Sines 7952 I Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/11/1207:21 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 LablD: C 12090481-004 Client Sample ID: TW4-06_09112012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit.. Result 21 0.1 ND 6.9 ND ND 115 138 129 112 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier RL D 2 0.1 1.0 1.0 1.0 1.0 80-120 S 70-130 S 80-120 80-120 MCL! QCL Method E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B MCl -Maximum contaminant level. Analysis Date 1 By 09/17/1223:101 wc 09/17/1214:37/1r 09/24/12 02:08 1 jk 09/24/1202:081 jk 09/24/12 02:08 1 jk 09/24/12 02:081 jk 09/24/12 02:081 jk 09/24/12 02:081 jk 09/24/12 02:081 jk 09/24/12 02:081 jk ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 6 of28 EN:RGY LABORATORIES www.energylab.com Analytical ExcsllsncB Sines 7852 Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/13/12 07:06 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Lab 10: C12090481-011 Client Sample 10: TW4-07_09132012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Report Defi nitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 40 3.B NO B70 NO NO 112 101 111 92.0 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier RL o 0.5 1.0 o 100 1.0 1.0 BO-120 70-130 BO-120 BO-120 MCL! QCL Method E300.0 E353.2 SWB260B SWB260B SWB260B SWB260B SWB260B SWB260B SWB260B SWB260B MCl -Maximum contaminant level. Analysis Date / By 09/1B/12 01 :12 1 wc 09/17/1215:07/1r 09/26/12 04:46 1 jk 09/27/12 00:561 jk 09/26/12 04:461 jk 09/26/12 04:46 1 jk 09/26/12 04:46 1 jk 09/26/1204:461 jk 09/26/12 04:46 1 jk 09/26/12 04:46 1 jk NO -Not detected at the reporting limit. Page 13 of 28 EN:RGY LABORATORIES www.energylab.com Analytical Ex~IIBflCI Sines '952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, 'NY 866-&86-1175 • Rapid City, SO 888-&12-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Lab 10: 3rd Quarter Chloroform Sampling 2012 C12081321-007 Client Sample 10: TW4-08_08292012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1 ,2-0ichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 48 0.1 NO NO NO NO 109 130 126 116 0-Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/12/12 Collection Date: 08/29/1209:25 DateReceived: 08/31/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By o 2 0.1 1.0 1.0 1.0 1.0 80-120 70-130 E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B 09/06/1222:431 wc 09/04/12 13:121 Ijl 09/04/12 23:201 jk 09/04/1223:201 jk 09/04/1223:201 jk 09/04/12 23:201 jk 09/04/12 23:201 jk 09/04/12 23:201 jk S 80-120 SW8260B 09/04/12 23:20 1 jk 80-120 SW8260B 09/04/12 23:201 jk MCl -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 9 of 23 EI\ERGY LABORATORIES WWIY.energyl a b.com Analytical ExcsllBflCfJ Sincs 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~illette, Wy 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Lab 10: 3rd Quarter Chloroform Sampling 2012 C12081321-008 Client Sample 10: TW4-09_08302012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: T 0luene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 22 3.9 NO NO NO NO 108 123 124 116 o -RL increased due to sample matrix. Units mg/L mg/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Report Date: 09/12/12 Collection Date: 08/30/1206:40 DateReceived: 08/31/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By o 0.2 1.0 1.0 1.0 1.0 80-120 70-130 E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B 09/06/12 23:00 1 wc 09/04/12 13:20 1 Ijl 09/04/12 23:551 jk 09/04/12 23:55 1 jk 09/04/12 23:551 jk 09/04/1223:551 jk 09/04/12 23:551 jk 09/04/12 23:551 jk S 80-120 SW8260B 09/04/12 23:551 jk 80-120 SW8260B 09/04/12 23:55 1 jk MeL -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 10 of 23 EN:RGY LABORAT ORIES www.energylab.com Anafytfca/ fusUsncfI Sines 79S2 Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/12/12 07:07 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Lab ID: C 12090481-007 Client Sample ID: TW4-10_09122012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 44 1.0 NO 130 NO NO 115 143 130 110 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC MCL! Qualifier Rl QCl Method Analysis Date 1 By o S S 0.1 1.0 10 1.0 1.0 80-120 70-130 80-120 80-120 E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B MCl -Maximum contaminant level. 09/18/1200:03/ wc 09/17/12 14:44/ Ir 09/24/12 03:54/ jk 09/24/12 04:29/ jk 09/24/1203:54/ jk 09/24/1203:54/ jk 09/24/12 03:54/ jk 09/24/12 03:54/ jk 09/24/12 03:54/ jk 09/24/12 03:54/ jk NO -Not detected at the reporting limit. S -Spike recovery outside of advisory 'limits. Page 9 of28 EI\ERGY LABORATORIES www.energylab.com Analytical ExcslfsncB Sines 1852 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Gasper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/13/12 06:57 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Lab ID: C12090481-010 Client Sample ID: TW4-11_09132012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Ch loromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-dS Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 49 3 ND 740 ND ND 114 100 114 91.0 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier RL D 1.0 D 100 1.0 1.0 SO-120 70-130 SO-120 SO-120 MCL! QCL Method E300.0 E353.2 SWS260B SWS260B SWS260B SWS260B SWS260B SWS260B SWS260B SWS260B MCl -Maximum contaminant level. Analysis Date 1 By 09/1S/12 00:551 wc 09/17/1215:04/Ir 09/26/12 04:10/ jk 09/27/1200:21 / jk 09/26/1204:10/ jk 09/26/12 04:101 jk 09/26/12 04:101 jk 09/26/12 04:101 jk 09/26/12 04:10/ jk 09/26/1204:10/ jk ND -Not detected at the reporting limit. Page 12 of28 EN:RGY l.ABORATORIES www.energylab.com Analytical ExCllOBflCB Sines 1!152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~illette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: LablD: 3rd Quarter Chloroform Sampling 2012 C12081321-003 Client Sample ID: TW4-12_08292012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 39 13 NO NO NO NO 106 121 125 116 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/12/12 Collection Date: 08/29/1206:45 DateReceived: 08/31/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date / By 0 S 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B MCl -Maximum contaminant level. 09/06/1220:241 wc 09/04/12 13:021 Ijl 09/04/1217:301 jk 09/04/12 17:301 jk 09/04/1217:301 jk 09/04/12 17:301 jk 09/04/12 17:301 jk 09/04/12 17:30 1 jk 09/04/12 17:301 jk 09/04/12 17:30 1 jk NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 5 of 23 EN:RGY L ABORATORIES www.energylab.com Analytical ExcsHencl Sincs 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Gasper, WY 888-235-0515 gillette, WY 86&-686-1175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: LablD: 3rd Quarter Chloroform Sampling 2012 C12081321-004 Client Sample ID: TW4-13_08292012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 60 6.2 ND ND ND ND 109 125 129 116 D -RL increased due to sample matrix. Units mg/L mg/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Report Date: 09/12/12 Collection Date: 08/29/1206:55 DateReceived: 08/31/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date / By D 1 0.5 1.0 1.0 1.0 1.0 80-120 70-130 E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B 09/06/12 21 :16 1 wc 09/04/1213:05/1jl 09/04/12 18:041 jk 09/04/12 18:041 jk 09/04/12 18:041 jk 09/04/12 18:041 jk 09/04/12 18 :04 1 jk 09/04/1218:04/jk S 80-120 SW8260B 09/04/1218:04/jk 80-120 SW8260B 09/04/12 18 :04 1 jk MCL -Maximum contaminant level. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 6 of 23 EN:RGY LABORATORIES www.energylab.com Analytical ExcsHBflCB Sincs 1m Helena, MT 877-472-0111 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 ~illette, Wy 86&-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: LablD: 3rd Quarter Chloroform Sampling 2012 C12081321-005 Client Sample ID: TW4-14_08292012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chlorom ethane Methylene chloride Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 37 3.9 ND ND ND ND 107 124 126 116 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/12/12 Collection Date: 08/29/12 07:06 DateReceived: 08/31/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By D D 2 0.2 1.0 1.0 1.0 1.0 80-120 70-130 E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B 09/06/12 22 :08 1 wc 09/04/12 13:07 1 Ijl 09/04/12 18:39 1 jk 09/04/12 18:39 1 jk 09/04/12 18:39 1 jk 09/04/1218:39/jk 09/04/12 18:391 jk 09/04/12 18:391 jk S 80-120 SW8260B 09/04/12 18:391 jk 80-120 SW8260B 09/04/12 18:391 jk MCl -Maximum contaminant level. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 7 of 23 EN:RGY LABORATORIES www.energylab.com Analytical ExCSUBflCfi/ Sines 1952 r-Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 J .. Gillette, 'IIY 866-68ti-7115 • Rapid COy, SD 888-612-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 LablD: C 12090222-005 Client Sample ID: MW-26_09042012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 73 2.6 ND 3100 ND 31 116 151 137 129 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl D 2 0.1 1.0 D 50 1.0 1.0 80-120 S 70-130 S 80-120 S 80-120 Report Date: 09/25/12 Collection Date: 09/04/12 13:50 DateReceived: 09/07/12 Matrix: Aqueous MCL/ QCl Method E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B Analysis Date 1 By 09/11/12 21 :32 1 wc 09/10/12 11 :21 1 Ir 09/11/1219:591 jk 09/13/12 17:441 jk 09/11/1219:591 jk 09/11/1219:591 jk 09/11/1219:591 jk 09/11/1219:591 jk 09/11/12 19:591 jk 09/11/1219:591 jk MCl -Maximum contaminant level. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 7 of 19 EN:RGY LABORATORIES www.energylab.com Analytical ExCBUBflCII Sincs 1m r Helena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~ilIette, Wy 86&-686-1175 • Rapid City, SD 888-672-1225 • College Station, lX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Lab 10: 3rd Quarter Chloroform Sampling 2012 C12081321-009 Client Sample 10: TW4-16_08302012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: T 0luene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 59 NO NO NO NO NO 110 133 128 117 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl o 2 0.1 1.0 1.0 1.0 1.0 80-120 S 70-130 S 80-120 80-120 Report Date: 09/12/12 Collection Date: 08/30/1206:50 DateReceived: 08/31/12 Matrix: Aqueous MCLI QCl Method E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B Analysis Date / By 09/06/1223:181 wc 09/04/12 13:27 1 Ijl 09/07/12 17:11 1 jk 09/07/12 17:11 1 jk 09/07/12 17:11 1 jk 09/07/12 17:11 1 jk 09/07/1217:11/jk 09/07/1217:11 1 jk 09/07/12 17:11 1 jk 09/07/12 17:11 1 jk Mel -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 11 of 23 EI'ERGY LABORAT ORIES www;energylab.com Analytical ExCBIIBflCfI Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 fI Casper, WV 888-235-0515 Gillette, WY 866-686-1175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Lab ID: C 12090222-002 Client Sample ID: MW-32_09052012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Report Definitions: Rl -Analyte reporting limit. QCL -Quality control limit. Result 33 NO NO NO NO NO 119 157 13B 12B o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl o 2 0.1 1.0 1.0 1.0 1.0 BO-120 S 70-130 S BO-120 S BO-120 Report Date: 09/25/12 Collection Date: 09/05/12 13:40 DateReceived: 09/07/12 Matrix: Aqueous MCL! QCl Method E300.0 E353.2 SWB260B SWB260B SWB260B SWB260B SWB260B SWB260B SWB260B SWB260B Analysis Date 1 By 09/11/12 19:301 wc 09/10/12 11 :13 /lr 09/11/121B:13/jk 09/11/121B:13/jk 09/11/12 1B:13 1 jk 09/11/12 1B:13 1 jk 09/11/121B:13/jk 09/11/121B:13/jk 09/11/12 1B:13 1 jk 09/11/12 1B:13 1 jk MCl -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 4 of 19 EN:RGY LABORATORIES www.energylab.com r Analytical Exesllsoes Sines 1952 ) Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/11/1207:47 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 LablD: C 12090481-006 Client Sample ID: TW4-18_09112012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: T 0luene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 26 6.6 ND 38 ND ND 117 137 132 110 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl D 1 0.5 1.0 1.0 1.0 1.0 80-120 S 70-130 S 80-120 80-120 MCL! . QCl Method E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B MCl -Maximum contaminant level. Analysis Date 1 By 09/17/1223:451 wc 09/17/1214:42/1r 09/24/12 03:191 jk 09/24/12 03:191 jk 09/24/12 03:191 jk 09/24/12 03: 19 1 jk 09/24/12 03:191 jk 09/24/12 03:191 jk 09/24/12 03:191 jk 09/24/12 03:191 jk ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 80f28 www.energylab.com Analytical ExcsJIBflCfJ Since 7952 ~ Helena, MT 877-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 J' , Gillette, WY 8&&-68&-7115 • Rapid City, SD 888-672-1225 • College Station, TJ( 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Lab 10: C12090222-001 Client Sample 10: TW4-19_09052012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: T 0luene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 149 2.5 3.5 950 NO NO 116 146 138 127 0-RL increased due to sample matrix. Units mg/L mg/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Qualifier RL 0.1 1.0 o 10 1.0 1.0 80-120 S 70-130 S 80-120 S 80-120 Report Date: 09/25/12 Collection Date: 09/05/12 10:40 DateReceived: 09/07/12 Matrix: Aqueous MCL! QCl Method E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B Analysis Date 1 By 09/11/1219:12/wc 09/10/12 11 :11 fir 09/11/1217:38/ jk 09/12/12 16:03/ jk 09/11/1217:38/ jk 09/11/1217:38/ jk 09/11/1217:38/ jk 09/11/1217:38/ jk 09/11/1217:38/ jk 09/11/1217:38/ jk MCL -Maximum contaminant level. NO - Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 3 of 19 EN:RGY LABORATORIES www.energylab.com Analytical uCBnsnce Since 71152 Helena, MT 877-412-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~iIIette, WY 86&-686-7115 • Rapid City, SD 888-612-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Lab 10: C 12090222-006 Client Sample 10: TW4-20_09042012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 289 10.8 26 13000 NO NO 115 137 142 138 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl o o 4 0.5 1.0 o 250 1.0 1.0 80-120 S 70-130 S 80-120 S 80-120 Report Date: 09/25/12 Collection Date: 09/04/12 13:35 DateReceived: 09/07/12 Matrix: Aqueous MCL/ QCl Method E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B Analysis Date 1 By 09/11/1221 :49 / wc 09/1 0112 11 :23 / Ir 09/11/1220:34/ jk 09/14/12 17:00 / jk 09/11/12 20:34/ jk 09/11/1220:34/ jk 09/11/1220:34/ jk 09/11/12 20:341 jk 09/11/1220:341 jk 09/11/1220:341 jk MCl -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 8 of 19 EN:RGY LABORATORIES www.energylab.com Analytical ExcsUsnCB Sines 7952 Helena, MT 817 -472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-1175 • Rapid City, SD 888-612-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/13/1206:45 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 LablD: C 12090481-009 Client Sample ID: TW4-21_09132012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-dS Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 142 13 6.0 410 ND ND 111 9S.0 112 92.0 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl D D 2 2 1.0 D 100 1.0 1.0 SO-120 70-130 SO-120 SO-120 MCL! QCl Method E300.0 E353.2 SWS260B SWS260B SWS260B SWS260B SWS260B SWS260B SWS260B SWS260B MCl -Maximum contaminant level. Analysis Date / By 09/1S/12 00:37 1 wc 09/17/12 14:57 1 Ir 09/26/1203:341 jk 09/26/12 23:461 jk 09/26/12 03:341 jk 09/26/12 03:341 jk 09/26/12 03:341 jk 09/26/12 03:341 jk 09/26/1203:341 jk 09/26/1203:341 jk ND -Not detected at the reporting limit. Page 11 of 28 EN:RGY LABORATORIES www.energylab.com Analytical Exes/lance Sines 7952 Helena, MT 877 -472-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/12/12 07:22 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 LablD: C 12090481-008 Client Sample ID: TW4-22_09122012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. OCl -Quality control limit. Result 121 7 NO 940 NO NO 108 98.0 109 93.0 0-Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl 0 1.0 0 100 1.0 1.0 80-120 70-130 80-120 80-120 MCL! QCl Method E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B MCl -Maximum contaminant level. Analysis Date / By 09/1 8/12 00:201 wc 09/17/12 14:47 1 Ir 09/25/12 14:37 1 jk 09/23/12 04:44 1 jk 09/25/12 14:37 1 jk 09/25/12 14:37 1 jk 09/25/12 14:37 1 jk 09/25/12 14:37 1 jk 09/25/12 14:37 1 jk 09/25/12 14:37 1 jk NO -Not detected at the reporting limit. Page 10 of28 EN:RGY LABORATORIES www.energylab.com Analytical IxCBIIBflcfI Sincs 1!J52 Helena, MT 877 -472-0711 • Billings, MT 800-735-4489 • Casper, W'f 888-235-0515 ~illett~, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Lab ID: 3rd Quarter Chloroform Sampling 2012 C12081321-006 Client Sample ID: TW4-23_08292012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 46 NO NO NO NO NO 110 130 128 116 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/12/12 Collection Date: 08/29/1209:13 DateReceived: 08/31/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date I By o 2 0.1 1.0 1.0 1.0 1.0 80-120 70-130 E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B 09/06/12 22:26 1 wc 09/04/12 13: 10 /ljl 09/04/12 19:14 I jk 09/04/12 19:14 I jk 09/04/12 19:141 jk 09/04/1219:141 jk 09/04/1219:14/jk 09/04/1219:141 jk S 80-120 SW8260B 09/04/1219:14/jk 80-120 SW8260B 09/04/1219:14/jk MCl -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 8 of 23 EN:RGY L.ASORATORIES www.energylab.com Analytical ExCSUBflCB Sincs 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~illette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Lab 10: 3rd Quarter Chloroform Sampling 2012 C12081321-010 Client Sample 10: TW4-24_08302012 Analyses Result Units MAJOR IONS Chloride 489 mg/l Nitrogen, Nitrate+Nitrite as N 37" mg/l VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride ND ug/l Chloroform 1.1 ug/l Chloromethane ND ug/l Methylene chloride ND ug/l Surr: 1 ,2-Dichlorobenzene-d4 85.0 %REC Surr: Dibromofluoromethane 96.0 %REC Surr: p-Bromofluorobenzene 82.0 %REC Surr: Toluene-d8 95.0 %REC -The sample was received in the laboratory with a pH > 2. The pH was 5. Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. D -Rl increased due to sample matrix. Report Date: 09/12/12 Collection Date: 08/30/12 07:00 DateReceived: 08/31/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By D D 5 5 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B MCl -Maximum contaminant level. 09/06/12 23:351 wc 09/04/12 13:301 Ijl 09/05/12 01 :43 / jk 09/05/12 01 :43 / jk 09/05/12 01 :43 / jk 09/05/12 01 :43 / jk 09/05/12 01 :43 / jk 09/05/12 01 :43 / jk 09/05/12 01 :43 / jk 09/05/12 01 :43 / jk ND -Not detected at the reporting limit. Page 12 of 23 EI\ERGY LABORAT ORIES www.energylab.com Anafytical ExcsUsnce Sines 1652 Helena, MT 877-472-0711 • Billings, MT 800'-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/11/1206:50 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 LablD: C 12090481-002 Client Sample ID: TW4-25_09112012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCL -Quality control limit. Result 334 17 ND ND ND ND 114 136 129 112 D -Rl increased due to sample matrix. Units mg/L mg/L ug/L ug/l ug/l ug/l %REC %REC %REC %REC Qualifier RL D D 2 2 1.0 1.0 1.0 1.0 80-120 S 70-130 S 80-120 80-120 MCL! QCL Method E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B MCl -Maximum contaminant level. Analysis Date / By 09/17/1221 :26 1 wc 09/17/1214:32/1r 09/24/12 00:57 1 jk 09/24/12 00:57 1 jk 09/24/12 00:57 1 jk 09/24/12 00:57 1 jk 09/24/1200:571 jk 09/24/12 00:571 jk 09/24/12 00:57 1 jk 09/24/12 00:57 1 jk ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 4 of28 EN:RGY LABORATORIES www.energylab.com Analytical Excsllsocs Sines 7852 Helena, MT 877 -472-0111 • Billings, MT 8IlB-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/10/12 10:20 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Lab 10: C 12090481-00 1 Client Sample 10: TW4-25R_09102012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: T 0luene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result NO NO NO NO NO NO 113 121 128 110 Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Qualifier Rl 0.1 1.0 1.0 1.0 1.0 80-120 70-130 S 80-120 80-120 MCll QCl Method E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B MCl -Maximum contaminant level. Analysis Date 1 By 09/17/1221 :09 1 wc 09/17/1214:29/1r 09/24/12 00:221 jk 09/24/12 00:221 jk 09/24/12 00:221 jk 09/24/12 00:221 jk 09/24/12 00:221 jk 09/24/12 00:221 jk 09/24/12 00:221 jk 09/24/12 00:221 jk NO -Not detected at the reporting limit. Page 30f28 EI\ERGY LA BORAT O RIES www.energylab.com Analytical Exes/lance Sincs 7952 Helena, MT 877 -472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-612-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/11/1207:08 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Lab ID: C 12090481-003 Client Sample ID: TW4-26_09112012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: T 0luene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 19 9 NO 4.9 NO NO 117 138 132 110 0-Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC MCL! Qualifier RL QCL Method Analysis Date 1 By 0 0 S S 4 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B MCl -Maximum contaminant level. 09/17/1222:181 wc 09/17/1214:34/1r 09/24/12 01 :33 1 jk 09/24/12 01 :33 1 jk 09/24/12 01 :33 1 jk 09/24/12 01 :33 1 jk 09/24/12 01 :33 1 jk 09/24/12 01 :33 1 jk 09/24/12 01 :33 1 jk 09/24/12 01 :33 1 jk NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 5 of28 EN:RGY LABORATORIES www.energylab.com Analytical Ixf;SHlHICfl Sincs 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~illette, WY 866-686-7175 • Rapid City, S[} 888-672-1225 • College Station, lX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: LablD: 3rd Quarter Chloroform Sampling 2012 C12081321-011 Client Sample ID: TW4-27 _08302012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 21 37 NO NO NO NO 86.0 96.0 80.0 91.0 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/12/12 Collection Date: 08/30/12 07:12 DateReceived: 08/31/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date / By 0 0 5 5 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 E300.0 E353.2 SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B SW8260B MCl -Maximum contaminant level. 09/06/12 23:53/ wc 09/04/1213:32/ljl 09/05/1202:19/ jk 09/05/1202:19/ jk 09/05/1202:19/ jk 09/05/1202:19/ jk 09/05/12 02:19/ jk 09/05/1202:19/ jk 09/05/1202:19/ jk 09/05/1202:19/ jk NO - Not detected at the reporting limit. Page 13 of 23 EN:RGY LABORAT O RIES ~~ www.energylab.com ~~ Analytical Excsllsncs Sines 7952 Helena, MT 877 -4 72-1l711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Collection Date: 09/13/12 08:55 DateReceived: 09/14/12 Matrix: Aqueous Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 LablD: C12090481-014 Client Sample ID: TW4-60_09132012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: T oluene-dS Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result NO NO NO 2.4 NO NO 110 94.0 110 92.0 Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl 1 0.1 1.0 1.0 1.0 1.0 SO-120 70-130 80-120 80-120 MCL! QCl Method E300.0 E353.2 SWS260B SWS260B SWS260B SWS260B SWS260B SWS260B SWS260B SW8260B MCl -Maximum contaminant level. Analysis Date / By 09/1S/12 19:251 wc 09/17/1215:14/1r 09/26/12 06:331 jk 09/26/12 06:33 1 jk 09/26/1206:331 jk 09/26/1206:331 jk 09/26/12 06:331 jk 09/26/12 06:331 jk 09/26/12 06:331 jk 09/26/12 06:331 jk NO -Not detected at the reporting limit. Page 16 of 28 EN:RGY LABORAT ORIES www.energylab.com Analytical ExcsHBflCB Sincs 1952 Helena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 LablD: C 12090222-007 Client Sample ID: TW4-65_09052012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: T 0luene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 34 NO NO NO NO NO 118 136 141 125 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/25/12 Collection Date: 09/05/12 13:40 DateReceived: 09/07/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date / By 0 2 E300.0 09/11/1222:061 wc 0.1 E353.2 09/10/12 11 :26 1 Ir 1.0 SW8260B 09/13/12 18:541 jk 1.0 SW8260B 09/13/12 18:541 jk 1.0 SW8260B 09/13/12 18:541 jk 1.0 SW8260B 09/13/12 18:541 jk 80-120 SW8260B 09/13/12 18:541 jk S 70-130 SW8260B 09/13/12 18:541 jk S 80-120 SW8260B 09/13/12 18:541 jk S 80-120 SW8260B 09/13/12 18:541 jk MCl -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 9 of 19 EN:RGY LABORATORIES www.energylab.com Analytical E.xcsHsnCB Sines 7852 J Helena, MT 817 -472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-686-1175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 LablD: C12090481-015 Client Sample ID: TW4-70_09112012 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dS Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 343 16 ND 1.3 ND ND 120 159 137 126 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/28/12 Collection Date: 09/11/1206:50 DateReceived: 09/14/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date / By D 2 E300.0 09/1S/12 19:431 wc D 1 E353.2 09/17/1215:17/1r 1.0 SWS260B 09/23/12 03:331 jk 1.0 SWS260B 09/23/12 03:33 1 jk 1.0 SWS260B 09/23/12 03:331 jk 1.0 SWS260B 09/23/12 03:331 jk SO-120 SWS260B 09/23/12 03:331 jk S 70-130 SWS260B 09/23/1203:331 jk S SO-120 SWS260B 09/23/12 03:331 jk S SO-120 SWS260B 09/23/12 03:331 jk MCl -Maximum contaminant level. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 17 of 28 EN:RGY LABORATORIES ~~ www.energylab.com ~~ Analytical ExcallBflCB Sincs 1952 Helena, MT 877-472-071 t • Billings, MT 800-735-4489 . Casper, WV 888-235-0515 ~illette, WY 866-&86-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: LablD: 3rd Quarter Chloroform Sampling 2012 C12081321-012 Client Sample ID: Trip Blank 6746 Analyses VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chlorom ethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units NO ug/l NO ug/l NO ug/l NO ug/l 84.0 %REC 94.0 %REC 82.0 %REC 89.0 %REC Qualifier Rl 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Report Date: 09/12/12 Collection Date: 08/28/12 DateReceived: 08/31/12 Matrix: Aqueous MCL! QCl Method Analysis Date / By SW8260B 09/05/12 01 :06 1 jk SW8260B 09/05/12 01 :06 1 jk SW8260B 09/05/12 01 :06 1 jk SW8260B 09/05/12 01 :06 1 jk SW8260B 09/05/12 01 :06 1 jk SW8260B 09/05/12 01 :06 / jk SW8260B 09/05/12 01 :06 1 jk SW8260B 09/05/12 01 :06 / jk MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 14 of 23 EI\ERGY LABORATORiES www.energylab.com Analytical ExCSUBIICB Sines 1952 Helena, MT 877 -4 72-0711 • Billings, MT 800-735-4489 • Gasper, WY 888-235-0515 ~iIIette, WY 866-686-1115 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Energy Fuels Resources (USA) Inc 3rd Quarter Chloroform Sampling 2012 C12081321-013 Client Sample ID: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 3.0 Qualifier RL Report Date: 09/12/12 Collection Date: 08/30/12 DateReceived: 08/31/12 Matrix: Aqueous MCL! QCL Method Analysis Date / By E170.1 08/31/12 09 :55 / kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 15 of 23 EN:RGY LABORATORIES www.energylab.com Analytical ExCSnenCB Since 7952 Helena, MT 871-412-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~illette, WY 866-&86-7115 • Rapid City, SD 888-612-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 LablD: C 12090222-008 Client Sample ID: Trip Blank 6746 Analyses VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result NO NO NO NO 116 136 137 126 Units ug/l ug/l ug/l ug/l %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Report Date: 09/25/12 Collection Date: 09/04/12 DateReceived: 09/07/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date / By 1.0 SW8260B 09/11/12 17:021 jk 1.0 SW8260B 09/11/1217:021 jk 1.0 SW8260B 09/11/12 17:021 jk 1.0 SW8260B 09/11/1217:021 jk 80-120 SW8260B 09/11/1217:021 jk S 70-130 SW8260B 09/11/1217:021 jk S 80-120 SW8260B 09/11/1217:021 jk S 80-120 SW8260B 09/11/12 17:021 jk MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 19 www.energylab.com EN:RGY LABORATORIES Analytical ExcsfilfflCB Sincs 1952 r-Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 ) . ~illotte, W'f 866-&86-1175 • Rapid City, SD 888-172-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Lab 10: C 12090222-009 Client Sample 10: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2.8 Qualifier Rl Report Date: 09/25/12 Collection Date: 09/04/12 DateReceived: 09/07/12 Matrix: Aqueous MCL! QCl Method Analysis Date 1 By E170.1 09/07/1209:401 kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 11 of 19 EN:RGY L ABORATORIES www.energylab.com J Analytical Exestlsnell Sinell 1952 Helena, MT 877 -472-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-612-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Lab ID: C12090481-016 Client Sample ID: Trip Blank 6746 Analyses VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result NO NO NO NO 112 93.0 113 92.0 Units ug/l ug/l ug/l ug/l %REC %REC %REC %REC H -Analysis performed past recommended holding time. Report Date: 09/28/12 Collection Date: 09/10/12 DateReceived: 09/14/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By H 1.0 SW8260B . 09/26/12 14:241 jk H 1.0 SW8260B 09/26/12 14:241 jk H 1.0 SW8260B 09/26/12 14:241 jk H 1.0 SW8260B 09/26/12 14:241 jk H 80-120 SW8260B 09/26/12 14:241 jk H 70-130 SW8260B 09/26/12 14:241 jk H 80-120 SW8260B 09/26/12 14 :24 1 jk H 80-120 SW8260B 09/26/12 14:241 jk MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 18 of 28 EI\ERGY LABORATORIES www.energylab.com Analytical ExcsUsncll Sines 7952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-&86-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Revised Date: 10/25/12 Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Lab 10: C12090481-017 Client Sample 10: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2.4 Report Date: 09/28/12 Collection Date: 09/13/12 DateReceived: 09/14/12 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By E170.1 09/14/12 09:451 kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 19 of 28 EN:RGY LABORATORIES www.energylab.com Analytical ExesihHn:. Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 ~iII~tte, wY 866-686-7115 • Rapid City, Sf} 888-672-1225 • College Station, IX 888-690-2218 ANALYTICAL SUMMARY REPORT September 12, 2012 Energy Fuels Resources (USA) Inc 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C12081321 Quote 10: C2975 -Chloroform Sampling Project Name: 3rd Quarter Chloroform Sampling 2012 Energy Laboratories, Inc. Casper WY received the following 13 samples for Energy Fuels Resources (USA) Inc on 8/31/2012 for analysis. Sample ID Client Sample ID C12081321-001 TW4-03R_08282012 C12081321-002 TW4-03_08292012 C12081321-003 TW4-12_08292012 C12081321-004 TW4-13_08292012 C12081321-005 TW4-14_08292012 C12081321-006 TW4-23_08292012 C12081321-007 TW4-08_08292012 C12081321-008 TW4-09_08302012 C12081321-009 TW4-16_08302012 C12081321-010 TW4-24_08302012 C12081321-011 TW4-27 _08302012 C12081321-012 Trip Blank 6746 C12081321-013 Temp Blank Collect Date Receive Date Matrix 08/28/127:32 08/31/12 Aqueous 08/29/12 6:26 08/31/12 Aqueous 08/29/12 6:45 08/31/12 Aqueous 08/29/126:55 08/31/12 Aqueous 08/29/127:06 08/31/12 Aqueous 08/29/129:13 08/31/12 Aqueous 08/29/12 9:25 08/31/12 Aqueous 08/30/12 6:40 08/31/12 Aqueous 08/30/12 6:50 08/31/12 Aqueous 08/30/127:00 08/31/12 Aqueous 08/30/127:12 08/31/12 Aqueous 08/28/120:00 08/31/12 Aqueous 08/30/120:00 08/31/12 Aqueous Test E300.0 Anions Nitrogen, Nitrate + Nitrite SW8260B VQCs, Standard List Same As Above Same As Above Same As Above Same As Above Same As Above Same As Above Same As Above Same As Above Same As Above Same As Above SW8260B VQCs, Standard List Temperature The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: c3¥~ D uJeJ.~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.09.12 13:42:31 -06:00 Page 1 of 23 www.energylab.com Analytical £XCSllenclI Sines Ig52 Helena, MT B71 .. 412~0711 • Billings, MT 800~735-4489 • Casper, WY 888~235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 CLIENT: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform Sampling 2012 Report Date: 09/12/12 Sample Delivery Group: C12081321 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-cs -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 23 EN:RGY LABORATORIES www.energylab.com Analytical £XCIII/snclI Sines 1952 Helena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 _ Gillette, WY 866-686-7115 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform Sampling 2012 Report Date: 09/12/12 Work Order: C12081321 Analyte Count Result Units RL %REC Low Limit High Limit Method: E300.0 Sample 10: ICV-090612-10 Chloride Method: E300.0 Sample 10: ICB-090612-11 Chloride Sample 10: LFB-090612-12 Chloride Sample 10: C12081321-004AMS Chloride Sample 10: C12081321-004AMSO Chloride Qualifiers: RL -Analyte reporting limit. Initial Calibration Verification Standard 9.66 mg/L 1.0 97 90 110 Method Blank Run: IC2-C_120906A NO mg/L 1.0 Laboratory Fortified Blank Run: IC2-C_120906A 9.83 mg/L 1.0 98 90 110 Sample Matrix Spike Run: IC2-C_120906A 110 mg/L 1.0 99 90 110 Sample Matrix Spike Duplicate Run: IC2-C_120906A 110 mg/L 1.0 99 90 110 NO -Not detected at the reporting limit. RPO RPOLimit Qual Analytical Run: IC2-C_120906A 09/06/12 12:16 0.3 Batch: R 164258 09/06/12 12:33 09/06/12 12:51 09/06/12 21 :33 09/06/1221 :51 10 Page 16 of 23 EN:RGY LABORATORIES www.energylab.com (' Analytical Exes/lancs Sines 1952 j Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~iIIeti:e, WY 86_6-686-7175 • Rapid City, SD 888-672-1225 • College Station, lX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform Sampling 2012 Analyte Count Result Units Method: E353.2 Sample 10: MBLK-1 Method Blank Nitrogen, Nitrate+Nitrite as N NO mg/L Sample 10: LCS-2 Laboratory Control Sample Nitrogen, Nitrate+Nitrite as N 2.55 mg/L Sample 10: LFB-3 Laboratory Fortified Blank Nitrogen, Nitrate+Nitrite as N 2.06 mg/L Sample 10: C12081321-o08BMS Sample Matrix Spike Nitrogen, Nitrate+Nitrite as N B.05 mg/L Sample 10: C12081321-008BMSO Sample Matrix Spike Duplicate Nitrogen, Nitrate+Nitrite as N 7.92 mg/L Qualifiers: RL -Analyte reporting limit. RL 0.10 0.10 0.10 0.20 0.20 Report Date: 09/12/12 Work Order: C12081321 %REC Low Limit High Limit RPO RPOLimit Qual Batch: R164101 Run: TECHNICON_120904A 09/04/12 11 :25 Run: TECHNICON_120904A 09/04/12 11 :27 102 90 110 Run: TECHNICON_120904A 09/04/12 11 :30 105 90 110 Run: TECHNICON_120904A 09/04/12 13:22 10B 90 110 Run: TECHNICON_120904A 09/04/12 13:25 105 90 110 1.6 10 NO -Not detected at the reporting limit. Page 17 of 23 EI\ERGY LABORAT ORIES www.energylab.com Analytical ExesllsnCB Sines 1952 r Helena, MT 877-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, lX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 09/12/12 Project : 3rd Quarter Chloroform Sampling 2012 Work Order: C12081321 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R164129 Sample 10: 04-Sep-12_LCS_ 4 8 Laboratory Control Sample Run: 5975VOC1_120904B 09/04/1213:17 Carbon tetrachloride 11 ug/L 1.0 110 70 130 Chloroform 9.9 ug/L 1.0 99 70 130 Chloromethane 16 ug/L 1.0 155 70 130 S Methylene chloride 9.7 ug/L 1.0 97 70 130 Surr: 1 ,2-Dichlorobenzene-d4 1.0 103 80 120 Surr: Dibromofluoromethane 1.0 112 70 130 Surr: p-Bromofluorobenzene 1.0 119 80 130 Surr: Toluene-d8 1.0 119 80 120 Sample 10: 04-Sep-12_MBLK_6 8 Method Blank Run: 5975VOC1 120904B 09/04/12 14:26 Carbon tetrachloride ND ug/L 1.0 Chloroform ND ug/L 1.0 Chloromethane ND ug/L 1.0 Methylene chloride ND ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 106 80 120 Surr: Dibromofluoromethane 1.0 111 70 130 Surr: p-Bromofluorobenzene 1.0 126 80 120 S Surr: Toluene-d8 1.0 115 80 120 Sample 10: C12081321-008CMS 8 Sample Matrix Spike Run: 5975VOC1 -120904B 09/04/12 20:24 Carbon tetrachloride 260 ug/L 10 129 70 130 Chloroform 230 ug/L 10 115 70 130 Chloromethane 270 ug/L 10 133 70 130 S Methylene chloride 220 ug/L 10 111 70 130 Surr: 1 ,2-Dichlorobenzene-d4 1.0 103 80 120 Surr: Dibromofluoromethane 1.0 120 70 130 Surr: p-Bromofluorobenzene 1.0 116 80 120 Surr: Toluene-d8 1.0 124 80 120 S Sample 10: C12081321-008CMSO 8 Sample Matrix Spike Duplicate Run: 5975VOC1 120904B 09/04/12 20:59 Carbon tetrachloride 230 ug/L 10 113 70 130 13 20 Chloroform 210 ug/L 10 105 70 130 9.1 20 Chloromethane 280 ug/L 10 140 70 130 5.3 20 S Methylene chloride 200 ug/L 10 98 70 130 12 20 Surr: 1 ,2-Dichlorobenzene-d4 1.0 104 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 113 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 117 80 120 0.0 10 Surr: Toluene-d8 1.0 122 80 120 0.0 10 S Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 18 of 23 EN:RGY LABORATO RIES www.energylab.com Analytical £XCIII/eneB Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 . ~illette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, 1X 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 09/12/12 Project: 3rd Quarter Chloroform Sampling 2012 Work Order: C12081321 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R164140 Sample 10: 090412_LCS_ 4 8 Laboratory Control Sample Run: SATURNCA_120904A 09/04/12 13:22 Carbon tetrachloride 9.3 ug/L 1.0 93 70 130 Chloroform 9.3 ug/L 1.0 93 70 130 Chloromethane 11 ug/L 1.0 109 70 130 Methylene chloride 8.8 ug/L 1.0 88 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 84 80 120 Surr: Dibromofluoromethane 1.0 87 70 130 Surr: p-Bromofluorobenzene 1.0 85 80 130 Surr: Toluene-d8 1.0 88 80 120 Sample 10: 090412_MBLK_6 8 Method Blank Run: SATURNCA_120904A 09/04/12 14:34 Carbon tetrachloride ND ug/L 1.0 Chloroform ND ug/L 1.0 Chloromethane ND ug/L 1.0 Methylene chloride ND ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 82 80 120 Surr: Dibromofluoromethane 1.0 86 70 130 Surr: p-Bromofluorobenzene 1.0 80 80 120 Surr: T 0luene-d8 1.0 91 80 120 Sample 10: C12081321-009CMS 8 Sample Matrix Spike Run: SATURNCA_120904A 09/04/1221 :28 Carbon tetrachloride 200 ug/L 10 98 70 130 Chloroform 200 ug/L 10 100 70 130 Chloromethane 220 ug/L 10 110 70 130 Methylene chloride 190 ug/L 10 97 70 130 Surr: 1 ,2-Dichlorobenzene-d4 1.0 81 80 120 Surr: Dibromofluoromethane 1.0 87 70 130 Surr: p-Bromofluorobenzene 1.0 79 80 120 S Surr: T 0luene-d8 1.0 91 80 120 Sample 10: C12081321-009CMSO 8 Sample Matrix Spike Duplicate Run: SATURNCA_120904A 09/04/1222:04 Carbon tetrachloride 200 ug/L 10 102 70 130 3.2 20 Chloroform 200 ug/L 10 101 70 130 0.8 20 Chloromethane 230 ug/L 10 116 70 130 5.3 20 Methylene chloride 200 ug/L 10 100 70 130 3.2 20 Surr: 1 ,2-Dichlorobenzene-d4 1.0 86 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 90 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 83 80 120 0.0 10 Surr: Toluene-d8 1.0 90 80 120 0.0 10 Qualifiers: RL -Analyte reporting limit. ND -Not detected.at the reporting limit. S -Spike recovery outside of advisory limits. Page 19 of 23 EN:RGY LABORAT ORIES www.energyJab.com Analytical Exesl/snell Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~illette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-221 a QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 09/12/12 Project: 3rd Quarter Chloroform Sampling 2012 Work Order: C12081321 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R164312 Sample 10: 07-Sep-12_LCS_ 4 8 Laboratory Control Sample Run: 5975VOC1_120907C 09/07/12 13:26 Carbon tetrachloride 12 ug/L 1.0 118 70 130 Chloroform 11 ug/L 1.0 109 70 130 Chloromethane 13 ug/L 1.0 126 70 130 Methylene chloride 10 ug/L 1.0 104 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 104 80 120 Surr: Dibromofluoromethane 1.0 115 70 130 Surr: p-Bromofluorobenzene 1.0 119 80 130 Surr: T oluene-d8 1.0 121 80 120 S Sample 10: 07-Sep-12_MBLK_6 8 Method Blank Run: 5975VOC1 120907C 09/07/12 14:36 Carbon tetrachloride ND ug/L 1.0 Chloroform ND ug/L 1.0 Chlorom ethane ND ug/L 1.0 Methylene chloride ND ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 105 80 120 Surr: Dibromofluoromethane 1.0 116 70 130 Surr: p-Bromofluorobenzene 1.0 125 80 120 S Surr: Toluene-d8 1.0 115 80 120 Sample 10: C12090159-006GMS 8 Sample Matrix Spike Run: 5975VOC1 120907C 09/07/1220:42 Carbon tetrachloride 280 ug/L 10 140 70 130 S Chloroform 250 ug/L 10 127 70 130 Chloromethane 260 ug/L 10 132 70 130 S Methylene chloride 230 ug/L 10 114 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 105 80 120 Surr: Dibromofluoromethane 1.0 126 70 130 Surr: p-Bromofluorobenzene 1.0 120 80 120 Surr: Toluene-d8 1.0 124 80 120 S Sample 10: C12090159-006GMSO 8 Sample Matrix Spike Duplicate Run: 5975VOC1 120907C 09/07/1221 :17 Carbon tetrachloride 270 ug/L 10 135 70 130 3.5 20 S Chloroform 250 ug/L 10 124 70 130 2.9 20 Chlorom ethane 250 ug/L 10 127 70 130 3.7 20 Methylene chloride _ 220 ug/L 10 110 70 130 3.2 20 Surr: 1 ,2-Dichlorobenzene-d4 1.0 104 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 119 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 118 80 120 0.0 10 Surr: T oluene-d8 1.0 123 80 120 0.0 10 S Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 20 of 23 EI\ERGY LASORAT ORI E:S tl!tJ'" www.energylab.com ~ Analytical £Zest/BIle, SiIlCB '952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~ille!te, Wy 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Kerri Schroeder Reviewed by: BL2000\alynch Reviewed Date: 9/4/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Temp Blank received? ContaineriT emp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0' Yes 0' Yes D Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' 3.0CC On Ice Yes 0' Yes 0' C12081321 Date Received: 8/31/2012 Received by: km Carrier NDA name: No D No D No D No D No D No D No D No D No D No D No D No D No D Not Present D Not Present D Not Present 0' Not Applicable D No VOA vials submitted D Not Applicable D Page 21 of 23 -u Q) co CD I'\) I'\) o -I'\) c.v Chain of Custody and Analytical Request Record Page --L-of --1- ---- ----- -'1.---- -------...... _ •••• _--_... --... --_ .. _.-•• Company Name: e(lU~ '::",elS Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: I 3f'~ ~\A~ .... +er ChJllrC+OrlY1 ~Ol~ State: u-J Yes¥ No D Report Mail Address: PO t3 '('j. Contact Name: Phone/Fax: Email: Sampler: (Please Print) . \ D 80q (T0..1'" r;f\ ?~",er '135 {;,7g .:22.:21 ~nne1"" ~-,I'J'ktf "5\{).n tA '(lq (AT SIi.5l1 Invoice Address: ~ ~ Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: D~v\~ ~r~ l.4~ ~8~1 Special Report/Formats: &00&11 W@D@ (]1rn®GD~§1ID .. Contact ELI prior to ~~;y: ~ RUSH sample submittal ~ Cl Q; C"ooler 10(s): ~o U).r:. LC) ~ R for charges and ~1XlJ5 01 Q; Q scheduling -See (,~t~JAi ._> 0 >-ro r--w t:, Instruction Page Dow D EOO/EDT(Electronic Data) ~(f.)~ m ~ 03:= ~ 0) ~ J: -C Receipt Temp o POTWNVWTP 0 c: Comments: Format: ~«~1.2~ ::::J U 3.6 "'fa 0 c <t 0 o State: o LEVEL IV o L.. all c: ~ '-•• CD c:.-~ m 1l ~ro~c l-e: CY Na, o Other: o NELAC .... On Ice: E~I~~ <t ::::J , l-S :J~:';:I8,o W 'E Custody Seal (/!' Z a. (I) ~ >1 ~ W m On Bottle en -C (f.) c: On Cooler 0 S H Intact N -S (f) SAMPLE IDENTIFICATION Collection Collection MATRIX '3 Signature Y N (Name, Location, Interval, etc.) Date Time Match 1 -r-vJ\.f-03 R_O&2.S20)~ g/~)!J. O"1~ 5-W .~ l~ 1-\\lY"'03_DgltJ~O;~ g/!:let Il!2.. OE.:t.& 5~W 'i ~ lywq-J.2..-082..'1 ~OIQ.. I g/~t1/j'J.. 0''-'5 ~-w y. g nnn ~w4-i3_og:t~X>12. S/:JAI'~ 06:b'5 ;-\\1 'I. ~ -N\f-) ~ _ Og~Cf2.0 12. 11/:J.~/tl.. 5-W . I~ 070, '/.. ~ J.r'W4 -.23_0g~cr ;to12 g/~q/)2. S-w . ~ O'lJ~ y.. 1'\\J Lf -OR .~;t '1.:2.0I!l. g/~'i/la... 0925 5-W 'J.. ~ J.r'W4" O'J~OgSO~ 12-W'lJ)/J2. 0'1.10 5-vJ '" ~ ~~ ... \L "«'~~Ol~ .U::!;D/J~ Ob~O 5-\,\). ~ I~ ~ ,,"\-..2.'i_08~;l,/) l:t SI~"~ 0700 ~-W .~ ~/;?Ogl&:<L 1c:J) Custody. ~:::ed~:)YIJlAtJ g/;'7D412. )100 _~~:u:: Jl U.J· I Received by (print): DatefTime: ' Signature: Record Relinquished by print): a Date/Time: Signafure: V Received by (print): Datemme: Signature: MUST be ~ Signed Recelvea DY LagalOry: l4::trme:~ J'it,lltft :SIgnature: Sample Disposal: Return to Client: lab Disposal: ".1l")l IfllTn ' '. In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. "'0 Q) co CD N c..v o -N c..v EN:RGY mJ-Chain of Custody and Analytical Request Record Page -2..-of -R-. ---....... -. .. "' ..... ,,--_ • -w .. ____ ................... ..." ......... ~ •• .,._ .... ___ ._ ..... , Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: State: Yes 0 No 0 I Report Mail Address: SrAf'Ylt Contact Name: <1D Phone/Fax: } Email: Sampler: (Please Print) I ~ ~ ~ -11~ I Invoice Address: '" ...",., Invoice Contact & Phone:-~ Purchase Order: Quote/Bottle Order: I - Special Report/Formats: 3: &00&[6 W@O@ OO@:@QJJ~(g[Q) ... Contact ELI prior to ~ 0 s-RUSH sample submittal ~O(/)~ ~ for charges and Cooler 10(s): ~al~OI Q) 0 R scheduling -See Cli~ ._> 0 ~m r'J w t:.. Instruction Page o DW 0 EDDJEDT(ElectronicData) ~en~ ~3: :c "0 Receipt Temp o POTWNJWTP Format: 03:= ro 0) U c: Comments: u«JSI.Q~ ~ :::::I U o .... mle: ~ 0 1o~~ °c o State: ·0 LEVEL IV •• <l) ~--(ij ~~ca.QQ \l l-e: CTN o Other: 0 NELAC ~Iro I L-On Ice: « ::I ::I Q).!: Q) s: %I l-S Z-a«Ig>o W "E Custody Seal f6 >1 ~ W co On Bottle e~ en "0 en c: On Cooler a:I .~ (j) H Intact SAMPLE IDENTIFICATION Collection Collection MATRIX ~ Signature (Name, Location, Interval, etc.) Date Time Match 1 ~ 11\\)'-\ -27_ ~f(~~Ot.:2. M/'V)JJ2 01J~ 5-W I~ J.rc'i~ ~k (~'1ql. f(/~j;l.. I~ 3 , . ..,. ~ nnn 4 ~ 5 I~ 6 ~ 7 ~ ~ 8 ~ .. 9 .~ 10 1./~ 8/ ~,;z.1 1c::J1 Custody jeli:~;:t\I~~ DatelTime: Signature: 11 /~L Received by (print): DateITime: Signa ure: ! iV:30/201!< noo ~ A ... -,.... ...., Record RelinqLlislied by (print): (J DatelTime: Signature: '-" Received by (print): DatelTime: Signature: MUST be Signed Sample Disposal: Return to Client: lab Disposal: Kecelvea Dy ':il':a~ry: I~ ;...t.;gJ8f I 'meu-~ JIll 'n,. ~tgnature: ~31 .. t.. cr~5 '" I I~ 1 ) V I:L .pI In certain circumstances, samples submitted to Energy Laboratories, Inc_ may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. EI\ERGY LABORATORIES www.energyJab.com Analytical ExCllIIsncB Sines 7952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-6B6-7175 • Rapid City, SD 888-672-1225 • College Station, lX 888-690-2218 ANALYTICAL SUMMARY REPORT September 25, 2012 Energy Fuels Resources (USA) Inc 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C12090222 Quote 10: C2975 -Chloroform Sampling Project Name: 3rd Quarter Chloroform 2012 Energy Laboratories, Inc. Casper WY received the following 9 samples for Energy Fuels Resources (USA) Inc on 9/7/2012 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C12090222-001 TW4-19_09052012 09105/12 10:40 09/07/12 Aqueous E300.0 Anions Nitrogen, Nitrate + Nitrite SW8260B VOCs, Standard List C 12090222-002 MW-32_09052012 09/05/12 13:40 09/07/12 Aqueous Same As Above C 12090222-003 MW -04_09042012 09/04/12 14:10 09/07/12 Aqueous Same As Above C 12090222-004 TW4-04_09042012 09/04/12 14:25 09/07/12 Aqueous Same As Above C 12090222-005 MW-26_09042012 09/04/12 13:50 09/07/12 Aqueous Same As Above C 12090222-006 TW4-20_09042012 09/04/12 13:35 09/07/12 Aqueous Same As Above C 12090222-007 TW4-65_09052012 09/05/12 13:40 09/07/12 Aqueous Same As Above C 12090222-008 Trip Blank 6746 09/04/12 0:00 09/07/12 Aqueous SW8260B VOCs, Standard List C 12090222-009 Temp Blank 09/04/120:00 09/07/12 Aqueous Temperature The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: cS¥~£) tJ~~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.09.25 15:40:18 -06:00 Page 1 of 19 www.energylab.com Analytical £XCIIllencs Sincs 1952 Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Ra id Ci ,SO 888-672-1225 • Colle e Station, IX 888-690-2218 CLIENT: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Report Date: 09/25/12 Sample Delivery Group: C12090222 CASE NARRATIVE ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4'C (±2'C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-cs ... Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 19 EI\ERGY LABORATORIES www.energylab.com Analytical Excellence Sines 1952 Helena, MT 877-472-011 1 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 QA/QC Su mmary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Report Date: 09/25/12 Work Order: C12090222 Analyte Count Result Units RL %REC Low Limit High Limit Method: E300.0 Sample 10: ICV-091112-10 Chloride Method: E300.0 Sample 10: ICB-091112-11 Chloride Sample 10: LFB-091112-12 Chloride Sample 10: C12090222-003AMS Chloride Sample 10: C12090222-003AMSO Chloride Qualifiers: RL -Analyte reporting limit. Initial Calibration Verification Standard 9.60 mg/L 1.0 96 90 110 Method Blank Run: IC1-C_120911A ND mg/L 1.0 Laboratory Fortified Blank Run: IC1 -C_120911A 10.1 mg/L 1.0 101 90 110 Sample Matrix Spike Run: IC1-C_120911 A 60.8 mg/L 1.0 97 90 110 Sample Matrix Spike Duplicate Run: IC1-C_120911A 61.4 mg/L 1.0 100 90 110 ND -Not detected at the reporting limit. RPO RPOLimit Qual Analytical Run: IC1-C_120911 A 09/11/12 11 :22 0.9 Batch: R164436 09/11/12 11 :40 09/11/12 11 :57 09/11/12 20:39 09/11/1220:57 10 Page 12 of 19 EI'-ERGY LABORATORIES www.energylab.com Analytical Excellence Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Analyte Count Result Units Method: E353.2 Sample 10: MBLK-1 Method Blank Nitrogen, Nitrate+Nitrite as N NO mg/L Sample 10: LCS-2 Laboratory Control Sample Nitrogen, Nitrate+Nitrite as N 2.51 mg/L Sample 10: LFB-3 Laboratory Fortified Blank Nitrogen, Nitrate+Nitrite as N 1.87 mg/L Sample 10: C12090218-0010MS Sample Matrix Spike Nitrogen, Nitrate+Nitrite as N 1.92 mg/L Sample 10: C12090218-0010MSO Sample Matrix Spike Duplicate Nitrogen, Nitrate+Nitrite as N 1.94 mg/L Qualifiers: RL -Analyte reporting limit. RL 0.10 0.10 0.10 0.10 0.10 Report Date: 09/25/12 Work Order: C 12090222 %REC Low Limit High Limit RPO RPOLimit Qual Batch: R164317 Run: TECHNICON_12091 OA 09/10/12 09:43 Run: TECHNICON_12091 OA 09/10/12 09:46 100 90 110 Run: TECHNICON_12091 OA 09/10/12 09:48 95 90 110 Run: TECHNICON_120910A 09/10/12 11 :03 98 90 110 Run: TECHNICON_12091 OA 09/10/12 11 :06 99 90 110 1.0 10 NO -Not detected at the reporting limit. Page 13 of 19 www.energylab.com Analytical Exesllence Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, W'f 888-235-0515 _Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 09/25/12 Project: 3rd Quarter Chloroform 2012 Work Order: C12090222 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R164457 Sample 10: 11-Sep_12_LCS_8 8 Laboratory Control Sample Run: 5975VOC1_120911A 09/11/12 13:28 Carbon tetrachloride 11 ug/L 1.0 113 70 130 Chloroform 11 ug/L 1.0 106 70 130 Chloromethane 9.1 ug/L 1.0 91 70 130 Methylene chloride 9.5 ug/L 1.0 95 70 130 Surr: 1 ,2-Dichlorobenzene-d4 1.0 112 80 120 Surr: Dibromofluoromethane 1.0 123 70 130 Surr: p-Bromofluorobenzene 1.0 128 80 130 Surr: Toluene-d8 1.0 129 80 120 S Sample 10: 11-Sep_12_MBLK_10 8 Method Blank Run: 5975VOC1 -120911A 09/11/1214:39 Carbon tetrachloride NO ug/L 1.0 Chloroform NO ug/L 1.0 Chloromethane NO ug/L 1.0 Methylene chloride NO ug/L 1.0 Surr: 1 ,2-Dichlorobenzene-d4 1.0 116 80 120 Surr: Dibromofluoromethane 1.0 128 70 130 Surr: p-Bromofluorobenzene 1.0 137 80 120 S Surr: T 0luene-d8 1.0 124 80 120 S Sample 10: C12090222-007CMS 8 Sample Matrix Spike Run: 5975VOC1 -120911A 09/11/12 21 :45 Carbon tetrachloride 290 ug/L 10 143 70 130 S Chloroform 340 ug/L 10 12 70 130 S Chloromethane 230 ug/L 10 113 70 130 Methylene chloride 260 ug/L 10 129 70 130 Surr: 1 ,2-Dichlorobenzene-d4 1.0 112 80 120 Surr: Dibromofluoromethane 1.0 150 70 130 S Surr: p-Bromofluorobenzene 1.0 127 80 120 S Surr: Toluene-d8 1.0 133 80 120 S -Target compound matrix carryover from previous samples caused interferance for the Chloroform recoveries in the MS/MSDo Sample 10: C12090222-007CMSO 8 Sample Matrix Spike Duplicate Run: 5975VOC1_120911A 09/11/12 22:20 Carbon tetrachloride 290 ug/L 10 145 70 130 1.1 20 S Chloroform 300 ug/L 10 -4 70 130 10 20 S Chloromethane 230 ug/L 10 116 70 130 2.4 20 Methylene chloride 250 ug/L 10 123 70 130 5.1 20 Surr: 1 ,2-Dichlorobenzene-d4 1.0 111 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 148 70 130 0.0 10 S Surr: p-Bromofluorobenzene 1.0 126 80 120 0.0 10 S Surr: Toluene-d8 1.0 131 80 120 0.0 10 S -Target compound matrix carryover from previous samples caused interferance for the Chloroform recoveries in the MS/MSD. __________________ 0 ____ 0 _______________________ 0 ____ 0 ____________________ 0 ___ 0._0.0 __________ 0 _______________ 0 __ _ Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 14 of 19 www.energylab.com Analytical Exes/lencs Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Gasper, WY 888-235-0515 ~illette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Analyte Count Result Units Method: SW8260B Sample 10: 12-Sep-12_LCS_ 4 Chloroform Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Sample 10: 12-Sep-12_MBLK_6 Chloroform Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Sample 10: C12090222-001 CMS Chloroform Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Sample 10: C12090222-001 CMSO Chloroform Surr: 1 ,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dB Qualifiers: RL -Analyte reporting limit. 5 Laboratory Control Sample B.B ug/L 5 Method Blank ND ug/L 5 Sample Matrix Spike 2300 ug/L 5 Sample Matrix Spike Duplicate 2300 ug/L S -Spike recovery outside of advisory limits. Report Date: 09/25/12 Work Order: C12090222 RL %REC Low Limit High Limit 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 50 1.0 1.0 1.0 1.0 50 1.0 1.0 1.0 1.0 Run: 5975VOC1_120912A BB 70 130 110 102 122 126 111 102 123 122 BO 70 BO BO 120 130 130 120 Run: 5975VOC1_120912A 80 70 BO BO 120 130 120 120 Run: 5975VOC1_120912A 103 70 130 109 119 126 125 109 109 119 125 126 BO 70 BO BO 120 130 120 120 Run: 5975VOC1_120912A 70 130 BO 120 70 BO BO 130 120 120 ND -Not detected at the reporting limit. RPO RPOLimit Qual 2.B 0.0 0.0 0.0 0.0 Batch: R164592 09/12/12 12:42 S 09/1211213:52 S S 09/12112 20:44 S S 09/1211221 :19 20 10 10 10 S 10 S Page 15 of 19 EI\ERGY LABORATORIES www.energylab.com Analytical Exesflsncil Sines 1152 Helena, MT 877-472-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 09/25/12 Project: 3rd Quarter Chloroform 2012 Work Order: C12090222 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R164597 Sample 10: 13-Sep-12_LCS_ 4 8 Laboratory Control Sample Run: 5975VOC1 _120913A 09/13/12 13:00 Carbon tetrachloride 11 ug/L 1.0 112 70 130 Chloroform 11 ug/L 1.0 106 70 130 Chlorom ethane 14 ug/L 1.0 140 70 130 S Methylene chloride 9.6 ug/L 1.0 96 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 112 80 120 Surr: Dibromofluoromethane 1.0 119 70 130 Surr: p-Bromofluorobenzene 1.0 126 80 130 Surr: Toluene-d8 1.0 129 80 120 S Sample 10: 13-Sep-12_MBLK_6 8 Method Blank Run: 5975VOC1 120913A 09/13/12 14:10 Carbon tetrachloride ND ug/L 1.0 Chloroform ND ug/L 1.0 Chlorom ethane ND ug/L 1.0 Methylene chloride ND ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 113 80 120 Surr: Dibromofluoromethane 1.0 123 70 130 Surr: p-Bromofluorobenzene 1.0 135 80 120 S Surr: Toluene-d8 1.0 124 80 120 S Sample 10: C12090222-007CMS 8 Sample Matrix Spike Run: 5975VOC1 120913A 09/13/1220:03 Carbon tetrachloride 280 ug/L 10 138 70 130 S Chloroform 250 ug/L 10 123 70 130 Chlorom ethane 330 ug/L 10 167 70 130 S Methylene chloride 240 ug/L 10 118 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 112 80 120 Surr: Dibromofluoromethane 1.0 132 70 130 S Surr: p-Bromofluorobenzene 1.0 127 80 120 S Surr: Toluene-d8 1.0 130 80 120 S Sample 10: C12090222-007CMSO 8 Sample Matrix Spike Duplicate Run: 5975VOC1 -120913A 09/13/12 20:39 Carbon tetrachloride 260 ug/L 10 131 70 130 5.6 20 S Chloroform 240 ug/L 10 122 70 130 1.3 20 Chlorom ethane 290 ug/L 10 145 70 130 14 20 S Methylene chloride 220 ug/L 10 111 70 130 6.3 20 Surr: 1,2-Dichlorobenzene-d4 1.0 110 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 137 70 130 0.0 10 S Surr: p-Bromofluorobenzene 1.0 128 80 120 0.0 10 S Surr: Toluene-d8 1.0 128 80 120 0.0 10 S Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 16 of 19 EN:RGY LABORATORIES www.energylab.com Analytical Exes/Janca Sines 1952 Helena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 . Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Report Date: 09/25/12 Project: 3rd Quarter Chloroform 2012 Work Order: C12090222 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R164602 Sample 10: 14-Sep-12_LCS_ 4 5 Laboratory Control Sample Run: 5975VOC1_120914A 09/14/12 11 :49 Chloroform 12 ug/L 1.0 118 70 130 Surr: 1 ,2-Dichlorobenzene-d4 1.0 110 80 120 Surr: Dibromofluoromethane 1.0 129 70 130 Surr: p-Bromofluorobenzene 1.0 126 80 130 Surr: T 0luene-d8 1.0 132 80 120 S Sample 10: 14-Sep-12_MBLK_6 5 Method Blank Run: 5975VOC1 120914A 09/14/12 12:59 Chloroform ND ug/L 1.0 Surr: 1 ,2-Dichlorobenzene-d4 1.0 113 80 120 Surr: Dibromofluoromethane 1.0 132 70 130 S Surr: p-Bromofluorobenzene 1.0 134 80 120 S Surr: T 0luene-d8 1.0 125 80 120 S Sample 10: C12090316-002KMS 5 Sample Matrix Spike Run: 5975VOC1 -120914A 09/14/12 20:31 Chloroform 110 ug/L 5.0 112 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 111 80 120 Surr: Dibromofluoromethane 1.0 116 70 130 Surr: p-Bromofluorobenzene 1.0 123 80 120 S Surr: T oluene-d8 1.0 130 80 120 S Sample 10: C12090316-002KMSO 5 Sample Matrix Spike Duplicate Run: 5975VOC1 120914A 09/14/12 21 :06 Chloroform 110 ug/L 5.0 106 70 130 5.9 20 Surr: 1 ,2-Dichlorobenzene-d4 1.0 110 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 110 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 122 80 120 0.0 10 S Surr: Toluene-d8 1.0 129 80 120 0.0 10 S Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 17 of 19 EN:RGY LABORATORIES ~JfJ'" .www.energyJab.com ~~ Analytic<llExcsllsncsSincs 1952 Helena, MT 877 -472-0711 -Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gilleife, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Timothy I.. Houghteling Reviewed by: BL2000\smead Reviewed Date: 9/10/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Temp Blank received? ContaineriTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes III Yes III Yes D Yes III Yes III Yes III Yes III Yes III Yes III Yes III Yes III 2.8"C On Ice Yes III Yes III C12090222 Date Received: 9/7/2012 Received by: km No D No D No D No D No D No D No D No D No D No D No D No D No D Carrier Next Day Ai r name: Not Present D Not Present D Not Present III Not Applicable D No VOA vials submitted D Not Applicable D Page 18 of 19 EN:RGY ~. Chain of Custody and Analytical Request Record Page_J _ofL ------------- --- -~ ---.,. ... ------......... ---------.----- Com pany Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: :Ener~ F"\J\e)s "3 r~ Q \A().I'~r C. h lorotd~ 2d'.< State: lA1"'" Yes ~ No 0 Report Mail Address: Contact Name: Phone/Fax: Email: Sampler: (Please Print) fo BoX 8D'\, BJA"J ~t\ tAT" 8YS/1 cr(Arrl~" Pal ""(:1" 1.""35 '78 ~:L~I ~ ner )/0) J, J'iJ: Invoice Address: Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: SW"C )7:) c:\ \) 1 A ·1 ""'("~ L.-135 ,,7,-za.J Special Report/Formats: ~&[b W®D® OOrn@(!D~§lID .. Contact ELI prior to 5hlpped by: S kLIh.,VM 0 Q; RUSH sample submittal for charges and CoolerlD{s): , ~o c/)..r:::: -R ~m~OI<u 0 ~ scheduling -See C/;ed ._> 0 >-10 W t::. I nstruction Page o DW 0 EDD/EDT(ElectronicData) Boo (J) m S L.i\ s:::: U3 (I) J: 03:= 1Q 0) '0 Recelp1Temp :rE~Z-o POTWNVWTP Format: t-O c:: Comments: u 00e ::I U ~ « Cl)liD1:.5;2 ~ « 0 :2.9 °c o State: D LEVEL IV o L-e '-... 0)$ C:-i:: ..... «t ~ Q.ml~ Cl ~ c:: (Y> o Other: 0 NELAC "-On Ice: ~<U • ::I .... -$ l-S ::I~<I~ ~ W -0 Custody Seal ZQ. Q)Cl fij >1 ~ W m On Bottle Y N en "C On Cool" S?: CI) c:: m ..... H Intact y -S CI) SAMPLE IDENTIFICATION Collection Collection MATRIX {3 Signature CJ N (Name, Location, Interval, etc.) Date Time Match 1 .s-w X "w'i-I'1 ... OqO~~O\'l. '1 /5/:J..O'~ 10LfO .~ 2J.\W_~ .OqO~U)~ '\/5/4.0'2 \~YO S-W :x. i~ 3 -~ 1--t/.2.0 I'l... J~'O 5-W )<. ~ JAW "0_11_ ()q 04!J..O l~ fln.n 4 JW4 "0'1--1l4 OLf:2.b~ ~/'i/.!J.Dj~ }L.f.2S S"'W ~ ~ 5 'MW-.2b.. DQD42.012 ~/'i/~)~ J350 ~ .. w )( !~ ~ 6 f1/a.vAO'~ \33.5 .!S-vJ ;< ~c I'A 0,0 ;;l)"'_~ TW~-UJ_O'Ul~2.012 7 Iq/.sl:z.bl~ &-w X ~ I 1\-J~ -_,};_ Oq 0 ~12 '3"'10 ~ 4(.;p B1An~ cP 1-'111 ,1..,/.101.2. ~ : ~~PlI1/1b I~ 10 'I ...... ' ' .. I~ Custody ~:~u~; bU~il~~.~ "t !'i;rr;~:J. ) 100 Signature: Ii JL:I _ Received by (print): DatelTime: Signa ure: Record ..::::J~ IT.,,,.," 1 Relinquished by (print): , DatelTime: Signature: V Received by (print): DatelTime: Signature: MUST be 1. Signed Sample Disposal: Return to Client: lab Disposal: I~ 1Vfiiu:;" Date'r/ 7 //Z t:'J~. "Itt ;:ilgnature: . In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. \ 1:-:" ~ •• -••• _'-_u~ ~ .... A ..... " ......... ",,1 ... 10. ........... f,.. .. ,:u~""iti,..n~1 infnrm~tinn rlnwnln~ri::lhIA fAA ~r.hP.rlIJIP.. forms_ and links. E~RGY LABORAT ORIES www.energylab.com f. Analytical ExcsUsncs Sines 1952 Helena, MT 877 .. 472-0711 • Billings, MT SnO-l35-tWS9 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 October 25,2012 Energy Fuels Resources (USA) Inc 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C12090481 ANAL VTICAL SUMMARY REPORT Quote ID: C2975 -Chloroform Sampling Project Name: 3rd Quarter Chloroform 2012 Energy Laboratories, Inc. Casper WY received the following 17 samples for Energy Fuels Resources (USA) Inc on 9/14/2012 for analYSis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C12090481-001 TW4-25R_09102012 09/10/12 10:20 09/14/12 Aqueous E300.0 Anions Nitrogen, Nitrate + Nitrite SW8260B VOCs, Standard List C 12090481-002 TW4-25_09112012 09/11/12 6:50 09/14/12 Aqueous Same As Above C 12090481-003 TW4-26_09112012 09/11/12 7:08 09/14/12 Aqueous Same As Above C 12090481-004 TW4-06_09112012 09/11/127:21 09/14/12 Aqueous Same As Above C12090481-005 TW4-05_09112012 09/11/127:35 09/14/12 Aqueous Same As Above C 12090481-006 TW4-18_09112012 09/11/127:47 09/14/12 Aqueous Same As Above C 12090481-007 TW4-10_09122012 09/12/12 7:07 09/14/12 Aqueous Same As Above C 12090481-008 TW4-22_09122012 09/12/12 7:22 09/14/12 Aqueous Same As Above C 12090481-009 TW4-21_09132012 09/13/12 6:45 09/14/12 Aqueous Same As Above C12090481-010 TW4-11_09132012 09/13/126:57 09/14/12 Aqueous Same As Above C12090481-011 TW4-07 _09132012 09/13/12 7:06 09/14/12 Aqueous Same As Above C12090481-012 TW4-01_09132012 09/13/127:17 09/14/12 Aqueous Same As Above C12090481-013 TW4-02_09132012 09/13/12 7:30 09/14/12 Aqueous Same As Above C12090481-014 TW4-60_09132012 09/13/12 8:55 09/14/12 Aqueous Same As Above C12090481-015 TW4-70_09112012 09/11/12 6:50 09/14/12 Aqueous Same As Above C12090481-016 Trip Blank 6746 09/10/120:00 09/14/12 Aqueous SW8260B VOCs, Standard List C12090481-017 Temp Blank 09/13/12 0:00 09/14/12 Aqueous Temperature The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: c3¥~D uJ~~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.10.25 13:52:29 ·06:00 Page 1 of28 www.energylab.com Analytical [xCSl/snell Sincs 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, 'NY 888-235-0515 Gillette, WY 866-686-7175 • Ra id Ci ,SD 888-672-1225 • College Station, TX 888-690-2218 CLIENT: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Sample Delivery Group: C12090481 REVISED/SUPPLEMENTAL REPORT (2) Revised Date: 10/25/12 Report Date: 09/28/12 CASE NARRATIVE The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on October 24, 2012 for the correction of the VOC's on sample -016. Due to the collection date change, the sample should have been flagged with an H flag. The data presented here is from that correction. REVISED/SUPPLEMENTAL REPORT (1) The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on September 28, 2012 to change the collection date on the Trip Blank to 9/10/12 and to add a collection date of 9/13/12 to the Temp Blank. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-cs -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of28 www.energylab.com AnafyticallxesllBI/CB Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Work Order: C12090481 Analyte Count Result Units RL %REC Low Limit High Limit Method: E300.0 Sample 10: ICV-091712-10 Chloride Method: E300.0 Sample 10: ICB-091712-11 Chloride Sample 10: LFB-091712-12 Chloride Sample 10: C12090481-003AMS Chloride Sample 10: C12090481-003AMSO Chloride Method: E300.0 Sample 10: ICV-091812-10 Chloride Method: E300.0 Sample 10: ICB-091812-11 Chloride Sample 10: LFB-091812-13 Chloride Sample 10: LFBO-091812-14 Chloride Sample 10: C12090560-001AMS Chloride Sample 10: C12090560-001AMSO Chloride Qualifiers: RL -Analyte reporting limit. Initial Calibration Verification Standard 9.78 mg/L 1.0 98 90 110 Method Blank Run: IC1-C_120917A ND mg/L 1.0 Laboratory Fortified Blank Run: IC1-C_120917A 9.78 mg/L 1.0 97 90 110 Sample Matrix Spike Run: IC1-C_1 20917A 214 mg/L 4.2 98 90 110 Sample Matrix Spike Duplicate Run: IC1-C_120917A 214 mg/L 4.2 98 90 110 Initial Calibration Verification Standard 9.56 mg/L 1.0 96 90 110 Method Blank Run: IC2-C_120918B ND mg/L 1.0 Laboratory Fortified Blank Run: IC2-C_120918B 9.48 mg/L 1.0 94 90 110 Laboratory Fortified Blank Duplicate Run: IC2-C_120918B 9.65 mg/L 1.0 96 90 110 Sample Matrix Spike Run: IC2-C_120918B 56.4 mg/L 1.0 102 90 110 Sample Matrix Spike Duplicate Run: IC2-C_120918B 56.2 mg/L 1.0 101 90 110 ND -Not detected at the reporting limit. RPO RPOLimit Qual Analytical Run: IC1 -C_120917A 09/17/1213:18 0.2 Batch: R164672 09/17/1213:36 09/17/12 13:53 09/17/1222:36 09/17/1222:53 10 Analytical Run: IC2-C_120918B 09/18/12 15:39 Batch: R164720 09/18/12 15:56 09/18/12 16:31 09/18/12 16:48 1.7 10 09/18/12 17:23 09/18/12 17:41 0.5 10 Page 20 of 28 EI\ERGY LABORATORIES '-rmN www.energylab.com Analytic8l ExesllBIICII Sines 7952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 10/25/12 Report Date: 09/28/12 Work Order: C12090481 Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Chloroform 2012 Analyte Count Result Units Method: E353.2 Sample 10: MBLK-1 Method Blank Nitrogen, Nitrate+Nitrite as N ND mg/L Sample 10: LCS-2 Laboratory Control Sample Nitrogen, Nitrate+Nitrite as N 2.41 mg/L Sample 10: LFB-3 Laboratory Fortified Blank Nitrogen, Nitrate+Nitrite as N 1.95 mg/L Sample 10: C12090481-009BMS Sample Matrix Spike Nitrogen, Nitrate+Nitrite as N 60.9 mg/L Sample 10: C12090481-009BMSO Sample Matrix Spike Duplicate Nitrogen, Nitrate+Nitrite as N 63.2 mg/L Qualifiers: RL -Analyte reporting limit. RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: R164662 Run: TECHNICON_120917B 09/17/1213:37 0.10 Run: TECHNICON_120917B 09/17/12 13:39 0.10 96 90 110 Run: TECHNICON_120917B 09/17/12 13:42 0.10 99 90 110 Run: TECHNICON_120917B 09/17/12 14:59 2.5 98 90 110 Run: TECHNICON_120917B 09/17/1215:02 2.5 103 90 110 3.7 10 ND -Not detected at the reporting limit. Page 21 of 28 EN:RGY LABORATORIES www.energylab.com Analytical best/snell Sines 1952 Helena, MT 877 -472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, Wy 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 10/25/12 Client: Energy Fuels Resources (USA) Inc Report Date: 09/28/12 Project: 3rd Quarter Chloroform 2012 Work Order: C12090481 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R164S75 Sample 10: 22-Sep-12_LCS_8 S Laboratory Control Sample Run: 5975VOC 1_120922A 09/22/12 12:52 Carbon tetrachloride 14 ug/L 1.0 142 70 130 S Chloroform 13 ug/L 1.0 134 70 130 S Chloromethane S.S ug/L 1.0 SS 70 130 Methylene chloride 12 ug/L 1.0 120 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 109 SO 120 Surr: Dibromofluoromethane 1.0 139 70 130 S Surr: p-Bromofluorobenzene 1.0 124 SO 130 Surr: Toluene-dS 1.0 12S SO 120 S Sample 10: 22-Sep-12_MBLK S Method Blank Run: 5975VOC1 120922A 09/22/12 14:02 Carbon tetrachloride ND ug/L 1.0 Chloroform ND ug/L 1.0 Chloromethane ND ug/L 1.0 Methylene chloride ND ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 117 SO 120 Surr: Dibromofluoromethane 1.0 132 70 130 S Surr: p-Bromofluorobenzene 1.0 133 SO 120 S Surr: T oluene-dS 1.0 125 SO 120 S Sample 10: C12090481-007CMS S Sample Matrix Spike Run: 5975VOC1 120922A 09/22/12 19:53 Carbon tetrachloride 2S0 ug/L 10 140 70 130 S Chloroform 390 ug/L 10 129 70 130 Chloromethane 210 ug/L 10 104 70 130 Methylene chloride 250 ug/L 10 127 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 110 SO 120 Surr: Dibromofluoromethane 1.0 14S 70 130 S Surr: p-Bromofluorobenzene 1.0 126 SO 120 S Surr: T oluene-dS 1.0 131 SO 120 S Sample 10: C12090481-007CMSO S Sample Matrix Spike Duplicate Run: 5975VOC1 120922A 09/22/12 20:2S Carbon tetrachloride 290 ug/L 10 144 70 130 2.5 20 S Chloroform 400 ug/L 10 132 70 130 1.S 20 S Chloromethane 240 ug/L 10 11S 70 130 12 20 Methylene chloride 270 ug/L 10 135 70 130 6.4 20 S Surr: 1,2-Dichlorobenzene-d4 1.0 111 SO 120 0.0 10 Surr: Dibromofluoromethane 1.0 146 70 130 0.0 10 S Surr: p-Bromofluorobenzene 1.0 125 SO 120 0.0 10 S Surr: Toluene-dS 1.0 129 SO 120 0.0 10 S Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 22 of28 EN:RGY LABORATORIES www;energyJab.com Analyticallxcsl/BlWB Sines 7952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 10/25/12 Client: Energy Fuels Resources (USA) Inc Report Date: 09/28/12 Project: 3rd Quarter Chloroform 2012 Work Order: C12090481 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R164887 Sample 10: 23-Sep-12_LCS_20 8 Laboratory Control Sample Run: 5975VOC1_120923A 09/23/12 22:01 Carbon tetrachloride 13 ug/L 1.0 126 70 130 Chloroform 12 ug/L 1.0 123 70 130 Chloromethane 9.4 ug/L 1.0 94 70 130 Methylene chloride 11 ug/L 1.0 110 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 109 80 120 Surr: Dibromofluoromethane 1.0 125 70 130 Surr: p-Bromofluorobenzene 1.0 118 80 130 Surr: Toluene-d8 1.0 116 80 120 Sample 10: 23-Sep-12_MBLK_22 8 Method Blank Run: 5975VOC1 -120923A 09/23/1223:11 Carbon tetrachloride ND ug/L 1.0 Chloroform ND ug/L 1.0 Chloromethane ND ug/L 1.0 Methylene chloride ND ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 113 80 120 Surr: Dibromofluoromethane 1.0 125 70 130 Surr: p-Bromofluorobenzene 1.0 128 80 120 S Surr: Toluene-d8 1.0 110 80 120 Sample 10: C12090481-007CMS 8 Sample Matrix Spike Run: 5975VOC1 120923A 09/24/12 05:04 Carbon tetrachloride 290 ug/L 10 144 70 130 S Chloroform 410 ug/L 10 139 70 130 S Chloromethane 190 ug/L 10 96 70 130 Methylene chloride 250 ug/L 10 127 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 108 80 120 Surr: Dibromofluoromethane 1.0 132 70 130 S Surr: p-Bromofluorobenzene 1.0 118 80 120 Surr: Toluene-d8 1.0 116 80 120 Sample 10: C12090481-007CMSO 8 Sample Matrix Spike Duplicate Run: 5975VOC1 120923A 09/24/12 05:40 Carbon tetrachloride 290 ug/L 10 144 70 130 0.6 20 S Chloroform 410 ug/L 10 140 70 130 0.6 20 S Chloromethane 240 ug/L 10 120 70 130 22 20 R Methylene chloride 250 ug/L 10 124 70 130 2.5 20 Surr: 1,2-Dichlorobenzene-d4 1.0 107 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 135 70 130 0.0 10 S Surr: p-Bromofluorobenzene 1.0 116 80 120 0.0 10 Surr: Toluene-d8 1.0 116 80 120 0.0 10 Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. R -RPD exceeds advisory limit. S -Spike recovery outside of advisory limits. Page 23 of 28 EN:RGY LABORAT ORIES www.energylab.com Analytical ExestlsoclI Sines 7952 Helena, MT 877-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7115 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 10/25/12 Client: Energy Fuels Resources (USA) Inc Report Date: 09/28/12 Project: 3rd Quarter Chloroform 2012 Work Order: C12090481 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R165011 Sample 10: 25-Sep-12_LCS_4 S Laboratory Control Sample Run: 5975VOC1_120925A 09/25/12 11 :21 Carbon tetrachloride 9.0 ug/L 1.0 90 70 130 Chloroform S.7 ug/L 1.0 S7 70 130 Chloromethane 15 ug/L 1.0 147 70 130 S Methylene chloride S.O ug/L 1.0 SO 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 106 SO 120 Surr: Dibromofluoromethane 1.0 90 70 130 Surr: p-Bromofluorobenzene 1.0 105 SO 130 Surr: Toluene-dS 1.0 97 SO 120 Sample 10: 25-Sep-12_MBLK_6 S Method Blank Run: 5975VOC1 -120925A 09/25/12 12:31 Carbon tetrachloride NO ug/L 1.0 Chloroform NO ug/L 1.0 Chloromethane NO ug/L 1.0 Methylene chloride NO ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 111 SO 120 Surr: Dibromofluoromethane 1.0 91 70 130 Surr: p-Bromofluorobenzene 1.0 112 SO 120 Surr: Toluene-dS 1.0 92 SO 120 Sample 10: C12090632-0040MS S Sample Matrix Spike Run: 5975VOC1 120925A 09/25/12 19:54 Carbon tetrachloride 200 ug/L 10 99 70 130 Chloroform 1S0 ug/L 10 92 70 130 Chloromethane 2S0 ug/L 10 142 70 130 S Methylene chloride 170 ug/L 10 S4 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 105 SO 120 Surr: Dibromofluoromethane 1.0 90 70 130 Surr: p-Bromofluorobenzene 1.0 104 SO 120 Surr: Toluene-dS 1.0 9S SO 120 Sample 10: C12090632-0040MSO S Sample Matrix Spike Duplicate Run: 5975VOC1 120925A 09/25/12 20:29 Carbon tetrachloride 200 ug/L 10 100 70 130 0.4 20 Chloroform 190 ug/L 10 95 70 130 3.0 20 Chloromethane 270 ug/L 10 136 70 130 4.6 20 S Methylene chloride 170 ug/L 10 S5 70 130 1.4 20 Surr: 1,2-Dichlorobenzene-d4 1.0 106 SO 120 0.0 10 Surr: Dibromofluoromethane 1.0 SS 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 104 SO 120 0.0 10 Surr: T oluene-dS 1.0 97 SO 120 0.0 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 24 of 2S EN:RGY LABORAT O RIES www.energylab.com Analytical ExeslllHlCB Sines '952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, lX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Revised Date: 10/25/12 Client: Energy Fuels Resources (USA) Inc Report Date: 09/28/12 Project: 3rd Quarter Chloroform 2012 Work Order: C12090481 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R165076 Sample 10: 26-Sep-12_LCS_4 S Laboratory Control Sample Run: 5975VOC1_120926A 09/26/12 10:57 Carbon tetrachloride 9.6 ug/L 1.0 96 70 130 Chloroform 9.4 ug/L 1.0 94 70 130 Chloromethane 13 ug/L 1.0 129 70 130 Methylene chloride S.7 ug/L 1.0 S7 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 106 SO 120 Surr: Dibromofluoromethane 1.0 S9 70 130 Surr: p-Bromofluorobenzene 1.0 104 SO 130 Surr: T oluene-dS 1.0 97 SO 120 Sample 10: 26-Sep-12_MBLK_6 S Method Blank Run: 5975VOC1 -120926A 09/26/12 12:07 Carbon tetrachloride NO ug/L 1.0 Chloroform NO ug/L 1.0 Chloromethane NO ug/L 1.0 Methylene chloride NO ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 111 SO 120 Surr: Dibromofluoromethane 1.0 91 70 130 Surr: p-Bromofluorobenzene 1.0 110 SO 120 Surr: Toluene-dS 1.0 92 SO 120 Sample 10: C12090481-015CMS S Sample Matrix Spike Run: 5975VOC1 120926A 09/26/12 19:39 Carbon tetrachloride 2200 ug/L 100 10S 70 130 Chloroform 2000 ug/L 100 101 70 130 Chloromethane 3000 ug/L 100 152 70 130 S Methylene chloride 1S00 ug/L 100 91 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 105 SO 120 Surr: Dibromofluoromethane 1.0 94 70 130 Surr: p-Bromofluorobenzene 1.0 104 SO 120 Surr: T oluene-dS 1.0 99 SO 120 Sample 10: C12090481-015CMSO S Sample Matrix Spike Duplicate Run: 5975VOC1 120926A 09/26/1220:15 Carbon tetrachloride 2100 ug/L 100 103 70 130 4.9 20 Chloroform 1900 ug/L 100 97 70 130 3.6 20 Chloromethane 2700 ug/L 100 134 70 130 12 20 S Methylene chloride 1700 ug/L 100 S5 70 130 7.3 20 Surr: 1,2-Dichlorobenzene-d4 1.0 105 SO 120 0.0 10 Surr: Dibromofluoromethane 1.0 91 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 102 SO 120 0.0 10 Surr: Toluene-dS 1.0 9S SO 120 0.0 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 25 of 28 EI\ERGY LABORATORIES ~JN www.energylab.com J . ~ Analytical Excsllence Sines 1852 . Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 86&-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Tracy Judge Reviewed by: BL2000\kmiller Reviewed Date: 9/19/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? . Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Temp Blank received? ContainerlT emp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 - Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 2.4OC On Ice Yes 0 Yes 0 C12090481 Date Received: 9/14/2012 Received by: km Carrier FedEx name: No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present III Not Applicable D No VOA vials submitted 0 Not Applicable D Page 26 of28 "'U III to CD N -..J Q, N ex> EI\ERGy m: m;J-Chain of Custody and Analytical Request Record Page~of~ Company Name: Proj~~t-Na';'~,--PWSr P~r~it-,-Etc. -.--_ .... -----.. _ •. _ •. --rr--s~~~i~ Origin EPA/State Compliance: £,A.(:,.t-.... ery ~ v~ I.!' :3 tc.l. 0 vo...r+cr L. L-\ C'>J'c)~ca-""", ~l;). State: uY Yes ~ No 0 Report Mait Address: P_O. ITo X (to q Contact Name: Phone/Fax: Email: Sampler: (Please Print) 131A.~'IA-!'::, I U, g4~t;j I Gtl--rrlA. PcJVV\.U ~1...S 67t ::l:;z.~l 1~e.rt+oll;J?--y Invoice Address: Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: 5~VV"-e...-5A,~L- Special Report/Formats: > ~ W@O@ rn3~®(!JJ~Lf~1ID .. Contact ELI prior to . ;IPperJ I:ly: .fNl.O I.~ ,l5 '-RUSH sample submittal l' Qd. --t.A.~.-". ~o (/) ~ -. for charges and Cooler 10(s): ~ CQ;g 01 CD O!;( R schedul ing -See O D 'B> ~ ~ ~ UJ t:., Instruction Page ("1 U ~ OW ' EDO/EDT(Electronic Data) c(f)~ ~;:> 'l..... I "0 ~ 0$:'-co 0> "I U c: C RecelptTemp D POTWIWWTP Format: U «~I.Q ~ f' :::l U omments: O State' D LEVEL IV ~ Q.L~~I,§ ~ ~ ~ ~.4 °c . E a. co 0 Cl '" ~ I-c I--======;"-';~-l D Other: D NELAC E~l~ I '-\ <t: :s On Ice: \VN :::l Q).-Q.) :s: I-5 z Q. «I ~Cl ~ UJ 'E Custody Seat ~ § >1 -\ W co On Bottle Y N (f) ~ (J) -g On Cooler fY"I ~ CO ~ ~ en H Intact ~ N SAMPLE IDENTIFICATION Collection Collection MATRIX A Signature (Name, Location, Interval, etc.) Date Time "'" Match N 1 TW"i· ?"1)~_ OqJ()~OI;z. CJ J ,oJ il.l 02D S -u "I I~ 2 'r W ~ -:L5 _ 0 q IL:2.0 j 2. q / jJ I J;" ();; S D 5 ~ w i I~ 3,0'-1-16_ ~qli~Oj.2.. q /11/1-2.. /')76 ~ _5 -W i ~ 4ru(,..I·06_DqIIW'~ q/II/1;1.... 07;;2./ s-W X ~ 5 TW"1-05_ O~,j ~o i ~ WIJ 1 a.. t} 735 _S ~ t.-J X I~ °rL ... ,..., .. ,,_ "qfl~,2. ClfuJr:l 071-./7 .5-W X' ~ 7,U/.1-10 Dql;l~I;2. QiJ2./la.. D707 5 ~ w 1-~ 8TW4-21._1)ctl:L~I~ qJI~"2 D7;"~ 5 -W X ~ 9'rw ~ -21_ 0 q t 3 MiA q j 11. J I 3.. /') 6 Li 5' 5 --W )( l~tJ ,ldtJtrf(/ 1~rw l-/-II-OCtJ320J;z.. Cf Ir3il:L 0657 5 -w f. ~t::::!l Custody Relinquished by (print): D atefTi me: / Sign~e: .-::> J Received by (print): Datemme: Signature: R d hl'A..rl'-M. PI-i.-v 1113;'7-1]00 6-~ t-"~. ecor Relinquished by (print): Datemme: Signature: Received by (print): Datemme: Signature: MUST be ' . V:ro_ oy l-I'?ffTnry: ~l' lime: ::>Ignawre: Signed Sample Disposal: Return to Client: Lab Disposal: r}l~ YJJiJllll.11/ ~\\L-I-\~~45 .. -. In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested, This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report, Visit our web site at www,energylab.com for additional information, downloadable fee schedule, forms, and links. 1-0 jill Pm N lex> 'a N lex> EI\ERGY m)'" Chain of Custody and Analytical Request Record Page ~ of ---2- t'Lt:A::>t: t't<IN I (prOVlae as much information as possible.) Company Name: Project Name, PWS, Permit. Etc. Sample Origin EPA/State Compliance: £, v'\.e.,r-3 i ~ u e.-l.J 3"'~ Qutu""teA" L:. l-\ 0 ,.. " (:' ~ (" ""'" ~VI~ State: VI Yes ~ No 0 Report Mail Address: Contact Name: Phone/Fax: Email: Sampler: (Please Print) P.O. 60)( £SOq &v..r('\,A.. .y(,)~1 If'""'. t.r 415 £7t6 2~~l -r"" ..... -~ ~bll;~~'1 g 1 t..A. el. ~ v':::~ 1 uT ('-IS' < Invoice Address: S ~."v'\.. L- Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: S~A/\..e- Special Report/Formats: :s: ~[1 W@D@ OOrn@l!D~rn@ + Contact ELI prior to rJ~bY~ Q Qj RUSH sample submittal ~O(/)£ for charges and Cooler 10($): ~Ol~OI Q.; Q S R scheduling -See ~ --> 0 >-ro ~Cf.)Cf.)rn$: W Instruction Page DDW D EDD/EDT(Electronic Data) c U5 (/) V) :::c -0s:= ~ 0') "C Receipt Temp o POTWNVWTP U c Comments: Format: u <t:b5lg ~ ,...... ::J U D State: o LEVEL IV '5 ... 001 c: ~ « e oJ.Ll DC ~~'*§(§ ~ ro c o Other: o NELAC ~~I~I ~ ~ :; On Ice: \!IN ::l (1)-: 1iJ S « l-S Zc..<CIg'O "# W "E Custody Seal @f> ~ >1 W m On Bottle en "0 (/J ,~ c: On Cooler m 0 N ... en H Intact ~ SAMPLE IDENTIFICATION Collection Collection MATRIX Signature <i/N (Name, Location, Interval, etc.) Date Time ~ Match 1 TW 1.../-0 7 _ O'll:!2012. ql,3/12 () 70/' 5-w i ~ 2 q iL:l/ I ~ 07\1 _C;~ W Y. ~ I:wJ../-O{ _ 0'1'3 20J;" 3 q/,:d;2 5 -l,;J 1-\Q1 rWL.I-O~_oqll~I'J... D730 Onn ~ .... ~ ~ ~ s '-'=' ru Lf-~{J_ Oq, 32011 ~ q J 13.J, :l. () 955 .5-W ~ 6 Cfjilll~ 5-~ ;< ~ rw Y .. 7D_ 0"1" 1.01 ;:t 0656 7 "l ~\ 0 tHI,l, h &1 tr~ I ~ 8 , ... -" ~ 01 9 lifo ~ 10 I~ Custody Relinquished by (print): DatelTime: Signature: ,J~ Received by (print): DatelTime: Signature: 6-17J":"'-f~J~ qiJ:lJ I).... / '-~ DO G~ PA -"'-"-_ Record Relinquished by (print): DatelTime: Signature: Received by (print): DatelTime: Signature: MUST be Signed ~ i!t:rr;aIDry: D~'I~~\~ ~~C& ~jgnature: Sample Disposal: Return to Client: Lab Disposal: In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. Tab I Quality Assurance and Data Validation Tables 1-1: Field QAlQC Evaluation 2x Casing Volume 2x Casing Volume Location Volume Pumped Volume Pumped Volume Check Conductivity RPD pH RPD Temp RPD Redox Potential RPD Turbidity RPD Continuously MW-4 NA pumped well --1961 . N/A 7.18 N/A 16.18 N/A 163 .N/A 0.0 N/A TW4-01 59.16 60.00 59 60 OK 2157 2153 0.19 6.29 6.29 0.00 14.69 14.68 0.07 247 . 245 0.81 140 .;,. M3 2.12 TW4-02 ·68.82 . 57.50 ' 69 58 ~pedDry 2921 . 2941 0,68 6.84 6.81 0.44 13.75 . ·13.8-3 0.58 262 260 0.77 6.9 8.3 18.42 TW4-03 118.60 90.00 119 90 . Pumped Dry 1589 J571 1.14 6.84 6.87 0.44 15.44 15.47 0.19 4J8 398 '.4.90 0 0 0.00 Continuously TW4-04 NA pumped well --2350 N/A 6.92 -"'. N/A 16.19 N/A 192 N/A 0 N/A TW4-05 82.68 90.00 83 90 OK 1489 1487 0.13 6.66 6.66 0.00 15.73 15.73 0.00 257 252 1.96 137 I·"; 140""",] 2.17 TW4-06 36.30 25.00 36 ' 25 Pumped Dry 3216 3207 0.28 6.3 6.4 1.57 14.56 14.56 0.00 449 425 5.49 0 . II s.f~ 200.00 TW4-07: 67.64 50.00. 68 50 Pumped Dry 1619 1631 0.74 7.15 7.09 0.84 13.85 13.87 0.14 249 . 250 0:40 8.6 9.3 "': 7.82 TW4-08 76.40 80.00 76 80 OK 3270 3270 0.00 6.91 6.95 0.58 15.54 15.54 0.00 75 75 0.00 100.6 .··.T00.1~ 0.50 TW4-09 85.46 90.00 85 90 OK 2323 2324 0.04 6.71 6.71 0.00 15.31 15.3 0.07 278 275 1.08 136 ·'~140 ··' 2.90 rW4-10 72.08 47.50 72 . 48 Pumped Dry,' 2416 ·2413 0.12 6.46 . 6.51 0.77 15 .79 15.73 . 0.38 246 248 . 0.81 . 7.9 7.8 1.27 TW4-11 56.28 60.00 56 60 OK 1612 1615 0.19 6.76 6.76 0.00 14.37 14.37 0.00 290 288 0.69 71 ·,'13 " 2.78 TW4-12 71.12 80.00 71 80 OK 1081 1080 0.09 6.59 6.58 0.15 15.11 15.07 0.27 450 ' 439 2.47 15.1 ti U.3 :. 1.32 TW4-13 72.22 . 55.00 72 55 Pumped Dry 1623 i620 0.19 7.18 7.2 0.28 15.06 15.12 0.40 337 328 2.71 0 0 0;00 TW4-14 8.42 5.00 8 5 Pumped Dry 3820 3800 0.52 7.34 7.4 0.81 14.82 '14.86 0.27 284 . 273 3.95 0 ·0 0.00 TW4-15 Continuously l (MW-26) NA pumped well --3438 N/A 6.79 N/A 15.48 N/A 176 N/A 0.00 N/A TW4-16 108.00 120.00 108 120 OK 3469 3473 0.12 6.66 6.68 0.30 15.43 15.39 0.26 127 130 2.33 38 ~u3j.h.£; 2.40 TW4-17 F . (MW-32) 73.20 73.78 73 74 OK 3825 3857 0.83 6.57 6.57 0.00 15.73 15.94 1.33 166 167 0.60 7 :< 'i.2." 2.82 TW4-18 104.86 110.00 105 110 OK 2073 2041 1.56 6.43 6.43 0.00 15.73 15.74 0.06 306 305 0.33 208 I{'~·~ '2'lL~ 1.43 Continuously TW4-19 NA pumped well --2816 N/A 6.96 N/A 15.45 N/A 322 N/A 0 N/A Continuously TW4-20 NA pumped well --4320 N/A 6.57 N/A 17.03 N/A 242 N/A 2.9 N/A TW4-21 86.94 90.00 87 90 OK 3506 3531 0.71 6.9 6.91 0.14 15.91 15.91 0.00 299 299 0.00 18 {)"8.'3 ~ .,~ 1.65 TW4-22 .. 78.98 67.50 79 68 Pumped Dry 1665 1670 '0.30 1.09 7.09 0.00 15.71 ·15:74 0.19 285 1. 286 . 0.35 1.6 1.8 11.76 TW4-23 64.56 70.00 65 70 OK 3644 3642 0.05 6.43 6.46 0.47 14.98 14.97 0.07 121 121 0.00 324 321 ~c 0.93 TW4-24 75.56 80.00 76 80 OK 9528 9545 0.18 6.68 6.71 0.45 15.56 15.54 0.13 235 230 2.15 4.8 ~'~.g . 2.11 TW4-25 111.78 120.00 112 120 OK 2951 2952 0.03 7.19 7.20 0.14 15.39 15.35 0.26 286 283 1.05 11.6 11.8 1.71 TW4..,26 29.84 . 17.50 30 18 Pumped Dry 628] 6276 0.08 4.39 4.42 .0.68 14.9 14.93 0.20 554 543 2.01 i6 . I~ lOtI 118.11 TW4-27 17.68 7.50. .18 8 Pumped Dry 5302 5279 0.43 7.06 7.01 0.71 16.05 16.32 1.67 359 353 1'.69 58.7 60.2 2.52 . MW-4, TW4-4, MW-26, TW,!-19, and TW4-20 are contmually umped.wegs. TW4-02,TW4-03, tW4-06, TW4-07, TW4-10, TW4-13, TW4-14" TW4..,22, TW4-26,'and TW4~27 were puniped dry andsampled after recovery. RPD > 10%. Per the revised QAP Revision 7.2, Attachment 2-3, when a well is purged to dryness, only pH, temperature and specific conductance parameters are required to be within 10% RPD. Redox potential and tmbidity parameters are measured for information purposes only and as such are not required to meet the 10% RPD criteria used for pH, specific conduc..:..::ta.:.:.:n:.:..ce=-a:.:.::.n:.::d....:.te.;,..m--!p!:..:e __ ra:.:.::.tur~e. ____ ----....--_---......-_------_-_~--_-----------,r-----------~--. The QAP states that turbidity should be less than 5 Nephelometric Turbidity Units ('~NTU") prior to sampling unless the well is characterizeM b1 water that has a higher turbidity. The Ql\P does not require tnat turbiClittr measm;,ements be less than 5 NTU rior to sam ling. A.s such the noted observations regardin turbidi!y measurements less than 5 N1U are included for information oses only. 1-2: Holding Time Evaluation Date Analysis Hold Time Allowed Hold Hold Time Location ID Parameter Name Sampled Date (Days) Time (Days) Check Trip Blank Carbon tetrachloride 8/28/2012 9/512012 8 14 OK Trip Blank Chloroform 8/28/2012 9/512012 8 14 OK Trip Blank Chloromethane 8/28/2012 9/512012 8 14 OK Trip Blank Methylene chloride 8/28/2012 9/512012 8 14 OK Trip Blank Carbon tetrachloride 9/4/2012 9111/2012 7 14 OK Trip Blank Chloroform 9/4/2012 9111/2012 7 14 OK Trip Blank Chloromethane 9/4/2012 9111/2012 7 14 OK Trip Blank Methylene chloride 9/4/2012 9111/2012 7 14 OK Trip Blank Carbon tetrachloride 9110/2012 9/26/2012 16 14 EXCEED Trip Blank Chloroform 911012012 9/26/2012 16 14 EXCEED Trip Blank Chloromethane 911012012 9/26/2012 16 14 EXCEED Trip Blank Methylene chloride 911012012 9/26/2012 16 14 EXCEED MW-04 Chloride 9/412012 9111/2012 7 28 OK MW-04 Carbon tetrachloride 9/4/2012 9111/2012 7 14 OK MW-04 Chloroform 9/4/2012 9113/2012 9 14 OK MW-04 Chloromethane 9/4/2012 9111/2012 7 14 OK MW-04 Methylene chloride 9/4/2012 9111/2012 7 14 OK MW-04 Nitrate + Nitrite as N 9/4/2012 9110/2012 6 28 OK MW-26 Chloride 9/4/2012 9111/2012 7 28 OK MW-26 Carbon tetrachloride 9/4/2012 9/11/2012 7 14 OK MW-26 Chloroform 9/4/2012 9/13/2012 9 14 OK MW-26 Chloromethane 9/4/2012 9111/2012 7 14 OK MW-26 Methylene chloride 9/4/2012 9111/2012 7 14 OK MW-26 Nitrate + Nitrite as N 9/4/2012 9110/2012 6 28 OK MW-32 Chloride 9/5/2012 9111/2012 6 28 OK MW-32 Carbon tetrachloride 9/5/2012 9111/2012 6 14 OK MW-32 Chloroform 9/5/2012 9111/2012 6 14 OK MW-32 Chloromethane 9/5/2012 9111/2012 6 14 OK MW-32 Methylene chloride 9/5/2012 9111/2012 6 14 OK MW-32 Nitrate + Nitrite as N 9/5/2012 9110/2012 5 28 OK TW4-01 Chloride 9113/2012 9118/2012 5 28 OK TW4-01 Carbon tetrachloride 9113/2012 9/26/2012 13 14 OK TW4-01 Chloroform 9113/2012 9/26/2012 13 14 OK TW4-01 Chloromethane 9113/2012 9/26/2012 13 14 OK TW4-01 Methylene chloride 9/13/2012 9/26/2012 13 14 OK TW4-01 Nitrate + Nitrite as N 9113/2012 9117/2012 4 28 OK TW4-02 Chloride 9113/2012 9118/2012 5 28 OK TW4-02 Carbon tetrachloride 9/13/2012 9/26/2012 13 14 OK TW4-02 Chloroform 9/13/2012 9/26/2012 13 14 OK TW4-02 Chloromethane 9/13/2012 9/26/2012 13 14 OK TW4-02 Methylene chloride 9/13/2012 9/26/2012 13 14 OK TW4-02 Nitrate + Nitrite as N 9113/2012 9117/2012 4 28 OK TW4-03 Chloride 8/29/2012 9/612012 8 28 OK TW4-03 Carbon tetrachloride 8/29/2012 9/412012 6 14 OK TW4-03 Chloroform 8/29/2012 9/412012 6 14 OK TW4-03 Chloromethane 8/29/2012 9/412012 6 14 OK TW4-03 Methylene chloride 8/29/2012 9/412012 6 14 OK TW4-03 Nitrate + Nitrite as N 8/29/2012 9/412012 6 28 OK 1-2: Holding Time Evaluation Date Analysis Hold Time Allowed Hold Hold Time Location ID Parameter Name . Sampled Date (Days) Time (Days) Check TW4-03R Chloride 8/28/2012 9/612012 9 28 OK TW4-03R Carbon tetrachloride 8/28/2012 9/7/2012 10 14 OK TW4-03R Chloroform 8/28/2012 9/7/2012 10 14 OK TW4-03R Chloromethane 8/28/2012 9/7/2012 10 14 OK TW4-03R Methylene chloride 8/28/2012 9/7/2012 10 14 OK TW4-03R Nitrate + Nitrite as N 8/28/2012 9/412012 7 28 OK TW4-04 Chloride 9/4/2012 9111/2012 7 28 OK TW4-04 Carbon tetrachloride 9/4/2012 9111/2012 7 14 OK TW4-04 Chloroform 9/4/2012 9113/2012 9 14 OK TW4-04 Chloromethane 9/4/2012 9111/2012 7 14 OK TW4-04 Methylene chloride 9/4/2012 9111/2012 7 14 OK TW4-04 Nitrate + Nitrite as N 9/4/2012 9110/2012 6 28 OK TW4-05 Chloride 9/11/2012 9117/2012 6 28 OK TW4-05 Carbon tetrachloride 9111/2012 9/24/2012 13 14 OK TW4-05 Chloroform 9/11/2012 9/24/2012 13 14 OK TW4-05 Chloromethane 9111/2012 9/24/2012 13 14 OK TW4-05 Methylene chloride 9111/2012 9/24/2012 13 14 OK TW4-05 Nitrate + Nitrite as N 9111/2012 9117/2012 6 28 OK TW4-06 Chloride 9111/2012 9117/2012 6 28 OK TW4-06 Carbon tetrachloride 9111/2012 9/24/2012 13 14 OK TW4-06 Chloroform 9111/2012 9124/2012 13 14 OK TW4-06 Chloromethane 9111/2012 9124/2012 13 14 OK TW4-06 Methylene chloride 9111/2012 9/24/2012 13 14 OK TW4-06 Nitrate + Nitrite as N 9111/2012 9117/2012 6 28 OK TW4-07 Chloride 9113/2012 9118/2012 5 28 OK TW4-07 Carbon tetrachloride 9113/2012 9/26/2012 13 14 OK TW4-07 Chloroform 9113/2012 9/27/2012 14 14 OK TW4-07 Chloromethane 9113/2012 9/26/2012 13 14 OK TW4-07 Methylene chloride 9113/2012 9/26/2012 13 14 OK TW4-07 Nitrate + Nitrite as N 9/13/2012 9117/2012 4 28 OK TW4-08 Chloride 8/29/2012 9/612012 8 28 OK TW4-08 Carbon tetrachloride 8/29/2012 9/412012 6 14 OK TW4-08 Chloroform 8/29/2012 9/412012 6 14 OK TW4-08 Chloromethane 8/29/2012 9/412012 6 14 OK TW4-08 Methylene chloride 8/29/2012 9/412012 6 14 OK TW4-08 Nitrate + Nitrite as N 8/29/2012 9/412012 6 28 OK TW4-09 Chloride 8/30/2012 9/612012 7 28 OK TW4-09 Carbon tetrachloride 8/30/2012 9/412012 5 14 OK TW4-09 Chloroform 8/30/2012 9/412012 5 14 OK TW4-09 Chloromethane 8/30/2012 9/412012 5 14 OK TW4-09 Methylene chloride 8/30/2012 9/412012 5 14 OK TW4-09 Nitrate + Nitrite as N 8/30/2012 9/412012 5 28 OK TW4-10 Chloride 9112/2012 9118/2012 6 28 OK TW4-10 Carbon tetrachloride 9112/2012 9/24/2012 12 14 OK TW4-10 Chloroform 9112/2012 9/24/2012 12 14 OK TW4-10 Chloromethane 9112/2012 9/24/2012 12 14 OK TW4-10 Methylene chloride 9112/2012 9/24/2012 12 14 OK TW4-10 Nitrate + Nitrite as N 9112/2012 9/17/2012 5 28 OK 1-2: Holding Time Evaluation Date Analysis Hold Time Allowed Hold Hold Time Location ID Parameter Name Sampled Date (Days) Time (Days) Check TW4-11 Chloride 9113/2012 9118/2012 5 28 OK TW4-11 Carbon tetrachloride 9113/2012 9/26/2012 13 14 OK TW4-11 Chloroform 9113/2012 9/27/2012 14 14 OK TW4-11 Chloromethane 9113/2012 9/26/2012 13 14 OK TW4-11 Methylene chloride 9113/2012 9/26/2012 13 14 OK TW4-11 Nitrate + Nitrite as N 9113/2012 9117/2012 4 28 OK TW4-12 Chloride 8/29/2012 9/612012 8 28 OK TW4-12 Carbon tetrachloride 8/29/2012 9/412012 6 14 OK TW4-12 Chloroform 8/29/2012 9/412012 6 14 OK TW4-12 Chloromethane 8/29/2012 9/412012 6 14 OK TW4-12 Methylene chloride 8/29/2012 9/412012 6 14 OK TW4-12 Nitrate + Nitrite as N 8/29/2012 9/412012 6 28 OK TW4-13 Chloride 8/29/2012 9/612012 8 28 OK TW4-13 Carbon tetrachloride 8/29/2012 9/412012 6 14 OK TW4-13 Chloroform 8/29/2012 9/412012 6 14 OK TW4-13 Chloromethane 8/29/2012 9/412012 6 14 OK TW4-13 Methylene chloride 8/29/2012 9/412012 6 14 OK TW4-13 Nitrate + Nitrite as N 8/29/2012 9/412012 6 28 OK TW4-14 Chloride 8/29/2012 9/612012 8 28 OK TW4-14 Carbon tetrachloride 8/29/2012 9/412012 6 14 OK TW4-14 Chloroform 8/29/2012 9/412012 6 14 OK TW4-14 Chloromethane 8/29/2012 9/412012 6 14 OK TW4-14 Methylene chloride 8/29/2012 9/412012 6 14 OK TW4-14 Nitrate + Nitrite as N 8/29/2012 9/412012 6 28 OK TW4-16 Chloride 8/30/2012 9/612012 7 28 OK TW4-16 Carbon tetrachloride 8/30/2012 9/7/2012 8 14 OK TW4-16 Chloroform 8/30/2012 9/7/2012 8 14 OK TW4-16 Chloromethane 8/30/2012 9/7/2012 8 14 OK TW4-16 Methylene chloride 8/30/2012 9/7/2012 8 14 OK TW4-16 Nitrate + Nitrite as N 8/30/2012 9/412012 5 28 OK TW4-18 Chloride 9111/2012 9117/2012 6 28 OK TW4-18 Carbon tetrachloride 9111/2012 9/24/2012 13 14 OK TW4-18 Chloroform 9111/2012 9124/2012 13 14 OK TW4-18 Chloromethane 9111/2012 9/24/2012 13 14 OK TW4-18 Methylene chloride 9111/2012 9/24/2012 13 14 OK TW4-18 Nitrate + Nitrite as N 9111/2012 9117/2012 6 28 OK TW4-19 Chloride 9/5/2012 9111/2012 6 28 OK TW4-19 Carbon tetrachloride 9/5/2012 9111/2012 6 14 OK TW4-19 Chloroform 9/5/2012 9112/2012 7 14 OK TW4-19 Chloromethane 9/5/2012 9111/2012 6 14 OK TW4-19 Methylene chloride 9/5/2012 9111/2012 6 14 OK TW4-19 Nitrate + Nitrite as N 9/5/2012 9110/2012 5 28 OK TW4-20 Chloride 9/4/2012 9111/2012 7 28 OK TW4-20 Carbon tetrachloride 9/4/2012 9111/2012 7 14 OK TW4-20 Chloroform 9/4/2012 9114/2012 10 14 OK TW4-20 Chloromethane 9/4/2012 9111/2012 7 14 OK TW4-20 Methylene chloride 9/4/2012 9111/2012 7 14 OK TW4-20 Nitrate + Nitrite as N 9/4/2012 9110/2012 6 28 OK 1-2: Holding Time Evaluation Date Analysis Hold Time Allowed Hold Hold Time Location ID Parameter Name Sampled Date (Days) Time (Days) Check TW4-21 Chloride 9113/2012 9118/2012 5 28 OK TW4-21 Carbon tetrachloride 9113/2012 9/26/2012 13 14 OK TW4-21 Chloroform 9113/2012 9/26/2012 13 14 OK TW4-21 Chloromethane 9113/2012 9/26/2012 13 14 OK TW4-21 Methylene chloride 9113/2012 9/26/2012 13 14 OK TW4-21 Nitrate + Nitrite as N 9/13/2012 9117/2012 4 28 OK TW4-22 Chloride 9112/2012 9118/2012 6 28 OK TW4-22 Carbon tetrachloride 9112/2012 9/25/2012 13 14 OK TW4-22 Chloroform 9112/2012 9/23/2012 11 14 OK TW4-22 Chloromethane 9112/2012 9/25/2012 13 14 OK TW4-22 Methylene chloride 9112/2012 9/25/2012 13 14 OK TW4-22 Nitrate + Nitrite as N 9112/2012 9117/2012 5 28 OK TW4-23 Chloride 8/29/2012 9/612012 8 28 OK TW4-23 Carbon tetrachloride 8/29/2012 9/412012 6 14 OK TW4-23 Chloroform 8/29/2012 9/412012 6 14 OK TW4-23 Chloromethane 8/29/2012 9/412012 6 14 OK TW4-23 Methylene chloride 8129/2012 9/4/2012 6 14 OK TW4-23 Nitrate + Nitrite as N 8/29/2012 9/412012 6 28 OK TW4-24 Chloride 8/30/2012 9/612012 7 28 OK TW4-24 Carbon tetrachloride 8/30/2012 9/512012 6 14 OK TW4-24 Chloroform 8/30/2012 9/512012 6 14 OK TW4-24 Chloromethane 8/30/2012 9/512012 6 14 OK TW4-24 Methylene chloride 8/30/2012 9/512012 6 14 OK TW4-24 Nitrate + Nitrite as N 8/30/2012 9/412012 5 28 OK TW4-25 Chloride 911112012 9117/2012 6 28 OK TW4-25 Carbon tetrachloride 911112012 9/24/2012 13 14 OK TW4-25 Chloroform 911112012 9/24/2012 13 14 OK TW4-25 Chloromethane 911112012 9/24/2012 13 14 OK TW4-25 Methylene chloride 911112012 9/24/2012 13 14 OK TW4-25 Nitrate + Nitrite as N 911112012 9117/2012 6 28 OK TW4-25R Chloride 9110/2012 9117/2012 7 28 OK TW4-25R Carbon tetrachloride 9110/2012 9/24/2012 14 14 OK TW4-25R Chloroform 9110/2012 9/24/2012 14 14 OK TW4-25R Chloromethane 9110/2012 9/24/2012 14 14 OK TW4-25R Methylene chloride 9110/2012 9124/2012 14 14 OK TW4-25R Nitrate + Nitrite as N 9110/2012 9117/2012 7 28 OK TW4-26 Chloride 911112012 9117/2012 6 28 OK TW4-26 Carbon tetrachloride 911112012 9/24/2012 13 14 OK TW4-26 Chloroform 911112012 9/24/2012 13 14 OK TW4-26 Chloromethane 911112012 9/24/2012 13 14 OK TW4-26 Methylene chloride 911112012 9/24/2012 13 14 OK TW4-26 Nitrate + Nitrite as N 911112012 9117/2012 6 28 OK TW4-27 Chloride 8/30/2012 9/612012 7 28 OK TW4-27 Carbon tetrachloride 8/30/2012 9/512012 6 14 OK TW4-27 Chloroform 8/30/2012 9/512012 6 14 OK TW4-27 Chloromethane 8/30/2012 9/512012 6 14 OK TW4-27 Methylene chloride 8/30/2012 9/512012 6 14 OK TW4-27 Nitrate + Nitrite as N 8/30/2012 9/412012 5 28 OK 1-2: Holding Time Evaluation Date Analysis Hold Time Allowed Hold Hold Time Location 1D Parameter Name Sampled Date (Days) Time (Days) Check TWN-60 Chloride 9/13/2012 9118/2012 5 28 OK TWN-60 Carbon tetrachloride 9113/2012 9/26/2012 13 14 OK TWN-60 Chloroform 9/13/2012 9/26/2012 13 14 OK TWN-60 Chloromethane 9113/2012 9/26/2012 13 14 OK TWN-60 Methylene chloride 9113/2012 9/26/2012 13 14 OK TWN-60 Nitrate + Nitrite as N 9113/2012 9117/2012 4 28 OK TW4-65 Chloride 9/5/2012 911112012 6 28 OK TW4-65 Carbon tetrachloride 9/5/2012 9/13/2012 8 14 OK TW4-65 Chloroform 9/5/2012 9113/2012 8 14 OK TW4-65 Chloromethane 9/5/2012 9113/2012 8 14 OK TW4-65 Methylene chloride 9/5/2012 9113/2012 8 14 OK TW4-65 Nitrate + Nitrite as N 9/5/2012 9110/2012 5 28 OK TW4-70 Chloride 911112012 9118/2012 7 28 OK TW4-70 Carbon tetrachloride 911112012 9/23/2012 12 14 OK TW4-70 Chloroform 911112012 9/23/2012 12 14 OK TW4-70 Chloromethane 911112012 9/23/2012 12 14 OK TW4-70 Methylene chloride 911112012 9123/2012 12 14 OK TW4-70 Nitrate + Nitrite as N 911112012 9117/2012 6 28 OK Table 1-3 Recipt Temperature Check Sample Batch Wells in Batch Temperature C12090481 TW4-2SR, TW4-2S, TW4-26, TW4-06, TW4-0S, TW4-18, 2.4 DC TW4-10, TW4-22, TW4-21, TW4-11, TW4-07, TW4-01, TW4-02, TW4-60, TW4-70, Trip Blank C12090222 TW4-19, MW-32, MW-04, TW4-04, MW-26, TW4-20, 2.8 DC TW4-6S, Trip Blank C12081321 TW4-03R, TW4-03, TW4-12, TW4-13, TW4-14, TW4-23, 3.0 DC TW4-08, TW4-09, TW4-16, TW4-24, TW4-27, Trip Blank I -4 Analytical Method Check Parameter Method Method Used byLab SW8260B or Carbon Tetrachloride SW8260C SW8260B A4500-CI B or A4500-CI E or Chloride E300.0 A4500-CI B SW8260B or Chlorofonn SW8260C SW8260B SW8260B or Chloromethane SW8260C SW8260B SW8260B or Methylene chloride SW8260C SW8260B Nitrogen E353.1 or E353.2 E353.2 All parameters were analyzed using the reporting method specificied in the QAP 15 R L· . Ch k -eportmg lImt ec Lab Required Reporting Reporting Location Analyte Limit Units Qualifier Limit . Units RL Check Trip Blank Carbon tetrachloride 1 ugiL U 1 ugIL OK Trip Blank Chloroform 1 ugIL U 1 ugIL OK Trip Blank Chloromethane 1 ugiL U 1 ugIL OK Trip Blank Methylene chloride 1 ugiL U 1 ugiL OK Trip Blank Carbon tetrachloride 1 ugIL U 1 ugIL OK Trip Blank Chloroform 1 ugiL U 1 ugIL OK Trip Blank Chloromethane 1 ugIL U 1 ugIL OK Trip Blank Methylene chloride 1 ugiL U 1 ugiL OK Trip Blank Carbon tetrachloride 1 ugIL UR 1 ugIL OK Trip Blank Chloroform 1 ugiL UH 1 ugIL OK Trip Blank Chloromethane 1 ugIL UR 1 ugiL OK Trip Blank Methylene chloride 1 ugiL UR 1 ugiL OK MW-04 Chloride 1 mgIL 1 mgIL OK MW-04 Carbon tetrachloride 1 ugIL 1 ugiL OK MW-04 Chloroform 50 ugiL D 1 ugiL OK MW-04 Chloromethane 1 ugiL U 1 ugIL OK MW-04 Methylene chloride 1 ugIL U 1 ugIL OK MW-04 Nitrate+Nitrite as N 0.5 ugIL D 0.1 ugIL OK MW-26 Chloride 2 mgIL D 1 mglL OK MW-26 Carbon tetrachloride 1 ugIL U 1 ugiL OK MW-26 Chloroform 50 ugIL D 1 ugIL OK MW-26 Chloromethane 1 ugIL U 1 ugIL OK MW-26 Methylene chloride 1 ugIL 1 ug/L OK MW-26 Nitrate+Nitrite as N 0.1 ugIL 0.1 ugiL OK MW-32 Chloride 2 mgIL D 1 mgIL OK MW-32 Carbon tetrachloride 1 ugIL U 1 ugiL OK MW-32 Chloroform 1 ugiL U 1 ug/L OK MW-32 Chloromethane 1 ugiL U 1 ugiL OK MW-32 Methylene chloride I ugIL U I ug/L OK MW-32 Nitrate+Nitrite as N 0.1 ugIL U 0.1 ugiL OK TW4-01 Chloride 1 mglL 1 mglL OK TW4-01 Carbon tetrachloride 1 ugiL U 1 ugiL OK TW4-01 Chloroform 100 ugIL D 1 ugiL OK TW4-01 Chloromethane 1 ugIL U 1 ug/L OK TW4-01 Methylene chloride 1 ugiL U 1 ugiL OK TW4-01 Nitrate+Nitrite as N 1 ugiL D 0.1 ugiL OK TW4-02 Chloride 2 mglL D 1 mgIL OK TW4-02 Carbon tetrachloride 1 ugiL 1 ugIL OK TW4-02 Chloroform 100 ugIL D 1 ugiL OK TW4-02 Chloromethane 1 ugIL U 1 ugIL OK TW4-02 Methylene chloride 1 ug/L U 1 ug/L OK TW4-02 Nitrate+ Nitrite as N 1 ug/L D 0.1 ug/L OK TW4-03 Chloride 1 mg/L 1 mg/L OK TW4-03 Carbon tetrachloride 1 ug/L U 1 ug/L OK TW4-03 Chloroform 1 ug/L U 1 ug/L OK TW4-03 Chloromethane 1 ug/L U 1 ug/L OK TW4-03 Methylene chloride 1 ugIL U 1 ug/L OK TW4-03 Nitrate+Nitrite as N 0.5 ug/L D 0.1 ug/L OK TW4-03R Chloride 1 mg/L U 1 mg/L OK TW4-03R Carbon tetrachloride 1 ugIL U 1 ugiL OK TW4-03R Chloroform 1 ugIL U 1 ug/L OK TW4-03R Chloromethane 1 ugIL U 1 ugIL OK TW4-03R Methylene chloride 1 ugIL U 1 ug/L OK TW4-03R Nitrate+Nitrite as N 0.1 ugiL U 0.1 ugiL OK 15 R L· . Ch k -eportmg lilllt ec Lab · Required . Reporting Reporting Location Analyte Limit Units Qualifier Limit Units RL Check TW4-04 Chloride 1 mglL 1 mgIL OK TW4-04 Carbon tetrachloride 1 ugiL 1 ugiL OK TW4-04 Chloroform 50 ugIL D 1 ug/L OK TW4-04 Chloromethane 1 ugIL U 1 ugIL OK TW4-04 Methylene chloride 1 ugIL U 1 ugIL OK TW4-04 Nitrate+Nitrite as N 0.2 ugIL D 0.1 ugIL OK TW4-05 Chloride 1 mgIL 1 mgIL OK TW4-05 Carbon tetrachloride 1 ugIL U 1 ugIL OK TW4-05 Chloroform 1 ugIL 1 ugIL OK TW4-05 Chloromethane 1 ugIL U 1 ugIL OK TW4-05 Methylene chloride 1 ugiL U 1 ugIL OK TW4-05 Nitrate+Nitrite as N 0.5 ugIL D 0.1 ugIL OK TW4-06 Chloride 2 mglL D 1 mglL OK TW4-06 Carbon tetrachloride 1 ugiL U 1 ugiL OK TW4-06 Chloroform 1 ugIL 1 ugiL OK TW4-06 Chloromethane 1 ugiL U 1 ugiL OK TW4-06 Methylene chloride 1 ugIL U 1 ugIL OK TW4-06 Nitrate+Nitrite as N 0.1 ugiL 0.1 ugiL OK TW4-07 Chloride 1 mgIL 1 mgIL OK TW4-07 Carbon tetrachloride 1 ugiL U 1 ugiL OK TW4-07 Chloroform 100 ugIL D 1 ugiL OK TW4-07 Chloromethane 1 ugIL U 1 ugIL OK TW4-07 Methylene chloride 1 ugiL U 1 ug/L OK TW4-07 Nitrate+Nitrite as N 0.5 ugIL D 0.1 ugIL OK TW4-08 Chloride 2 mgIL D 1 mgIL OK TW4-08 Carbon tetrachloride 1 ugiL U 1 ugiL OK TW4-08 Chloroform 1 ugIL U 1 ug/L OK TW4-08 Chloromethane 1 ugiL U 1 ug/L OK TW4-08 Methylene chloride 1 ugiL U 1 ugIL OK TW4-08 Nitrate+Nitrite as N 0.1 ug/L 0.1 ugiL OK TW4-09 Chloride 1 mglL 1 mgIL OK TW4-09 Carbon tetrachloride 1 ugIL U 1 ugIL OK TW4-09 Chloroform 1 ugiL U 1 ugIL OK TW4-09 Chloromethane 1 ugiL U 1 ugIL OK TW4-09 Methylene chloride 1 ugIL U 1 ug/L OK TW4-09 Nitrate+Nitrite as N 0.2 ugIL D 0.1 ugiL OK TW4-10 Chloride 1 mgIL 1 mgIL OK TW4-10 Carbon tetrachloride 1 ugIL U 1 ugIL OK TW4-10 Chloroform 10 ugIL D 1 ugIL OK TW4-10 Chloromethane 1 ugIL U 1 ugIL OK TW4-10 Methylene chloride 1 ug/L U 1 ugIL OK TW4-10 Nitrate+Nitrite as N 0.1 ug/L 0.1 ug/L OK TW4-11 Chloride 1 mglL 1 mglL OK TW4-11 Carbon tetrachloride 1 ug/L U 1 ug/L OK TW4-11 Chloroform 100 ug/L D 1 ug/L OK TW4-11 Chloromethane 1 ugIL U 1 ug/L OK TW4-11 Methylene chloride 1 ugIL U 1 ug/L OK TW4-11 Nitrate+Nitrite as N 1 ug/L D 0.1 ugiL OK TW4-12 Chloride 1 mglL 1 mglL OK TW4-12 Carbon tetrachloride 1 ugiL U I ugfL OK TW4-12 Chloroform 1 ugiL U 1 ugiL OK TW4-12 Chloromethane 1 ugIL U I ugiL OK TW4-12 Methylene chloride 1 ugIL U 1 ugiL OK TW4-12 Nitrate+Nitrite as N 1 ugIL D 0.1 ugIL OK 15 R L· . Ch k -eportmg lillit ec Lab Required _ Reporting Reporting Location Analyte Limit Units Qualifier Limit Units RL Check TW4-13 Chloride 1 mg/L 1 mg/L OK TW4-13 Carbon tetrachloride 1 ug/L U 1 ug/L OK TW4-13 Chloroform 1 ug/L U 1 ug/L OK TW4-13 Chloromethane 1 ug/L U 1 ug/L OK TW4-13 Methylene chloride 1 ug/L U 1 ug/L OK TW4-13 Nitrate+Nitrite as N 0.5 ug/L D 0.1 ug/L OK TW4-14 Chloride 2 mg/L D 1 mg/L OK TW4-14 Carbon tetrachloride 1 ug/L U 1 ug/L OK TW4-14 Chloroform 1 ug/L U 1 ug/L OK TW4-14 Chloromethane 1 ug/L U 1 ug/L OK TW4-14 Methylene chloride 1 ug/L U 1 ug/L OK TW4-14 Nitrate+Nitrite as N 0.2 ug/L D 0.1 ug/L OK TW4-16 Chloride 2 mg/L D 1 mg/L OK TW4-16 Carbon tetrachloride 1 ug/L U 1 ug/L OK TW4-16 Chloroform 1 ug/L U 1 ug/L OK TW4-16 Chloromethane 1 ug/L U 1 ug/L OK TW4-16 Methylene chloride 1 ug/L U 1 ug/L OK TW4-16 Nitrate+Nitrite as N 0.1 ug/L U 0.1 ug/L OK TW4-18 Chloride 1 mg/L 1 mg/L OK TW4-18 Carbon tetrachloride 1 ug/L U 1 ug/L OK TW4-18 Chloroform 1 ug/L 1 ug/L OK TW4-18 Chloromethane 1 ug/L U 1 ug/L OK TW4-18 Methylene chloride 1 ug/L U 1 ug/L OK TW4-18 Nitrate+Nitrite as N 0.5 ug/L D 0.1 ug/L OK TW4-19 Chloride 1 mg/L 1 mg/L OK TW4-19 Carbon tetrachloride 1 ug/L 1 ug/L OK TW4-19 Chloroform 10 ug/L D 1 ug/L OK TW4-19 Chloromethane 1 ug/L U 1 ug/L OK TW4-19 Methylene chloride 1 ug/L U 1 ug/L OK TW4-19 Nitrate+Nitrite as N 0.1 ug/L 0.1 ug/L OK TW4-20 Chloride 4 mg/L D 1 mg/L OK TW4-20 Carbon tetrachloride 1 ug/L 1 ug/L OK TW4-20 Chloroform 250 ug/L D 1 ug/L OK TW4-20 Chloromethane 1 ug/L U 1 ug/L OK TW4-20 Methylene chloride 1 ug/L U 1 ug/L OK TW4-20 Nitrate+Nitrite as N 0.5 ug/L D 0.1 ug/L OK TW4-21 Chloride 2 mg/L D 1 mg/L OK TW4-21 Carbon tetrachloride 1 ug/L 1 ug/L OK TW4-21 Chloroform 100 ug/L D 1 ug/L OK TW4-21 Chloromethane 1 ug/L U 1 ug/L OK TW4-21 Methylene chloride 1 ug/L U 1 ug/L OK TW4-21 Nitrate+Nitrite as N 2 ug/L D 0.1 ug/L OK TW4-22 Chloride 1 mg/L 1 mg/L OK TW4-22 Carbon tetrachloride 1 ug/L U 1 ug/L OK TW4-22 Chloroform 100 ug/L D 1 ug/L OK TW4-22 Chloromethane 1 ug/L U 1 ug/L OK TW4-22 Methylene chloride 1 ug/L U 1 ug/L OK TW4-22 Nitrate+Nitrite as N 1 ug/L D 0.1 ug/L OK TW4-23 Chloride 2 mg/L D 1 mg/L OK TW4-23 Carbon tetrachloride 1 ug/L U 1 ug/L OK TW4-23 Chloroform 1 ug/L U 1 ug/L OK TW4-23 Chloromethane 1 ug/L U 1 ug/L OK TW4-23 Methylene chloride 1 ug/L U 1 ug/L OK TW4-23 Nitrate+Nitrite as N 0.1 ug/L U 0.1 ug/L OK 15 R L· . Ch k -eportmg umt ec Lab Required Reporting Reporting Location Analyte Limit Units Qualifier Limit Units RL Check TW4-24 Chloride 5 mg/L D 1 mglL OK TW4-24 Carbon tetrachloride 1 ug/L U 1 ug/L OK TW4-24 Chloroform 1 ugiL 1 ug/L OK TW4-24 Chloromethane 1 ugiL U 1 ug/L OK TW4-24 Methylene chloride 1 ug/L U 1 ug/L OK TW4-24 Nitrate+Nitrite as N 5 ug/L D 0.1 ug/L OK TW4-25 Chloride 2 mglL D 1 mg/L OK TW4-25 Carbon tetrachloride 1 ugiL U 1 ugiL OK TW4-25 Chloroform 1 ug/L U 1 ug/L OK TW4-25 Chloromethane 1 ug/L U 1 ug/L OK TW4-25 Methylene chloride 1 ug/L U 1 ug/L OK TW4-25 Nitrate+Nitrite as N 2 ugiL D 0.1 ug/L OK TW4-25R Chloride 1 mg/L U 1 mglL OK TW4-25R Carbon tetrachloride 1 ugiL U 1 ug!L OK TW4-25R Chloroform 1 ugiL U 1 ug/L OK TW4-25R Chloromethane 1 ugiL U 1 ugiL OK TW4-25R Methylene chloride 1 ugiL U 1 ug/L OK TW4-25R Nitrate+Nitrite as N 0.1 ug/L U 0.1 ug/L OK TW4-26 Chloride 4 mg/L D 1 mg/L OK TW4-26 Carbon tetrachloride 1 ug/L U 1 ug/L OK TW4-26 Chloroform 1 ug/L 1 ug/L OK TW4-26 Chloromethane 1 ug/L U 1 ug/L OK TW4-26 Methylene chloride 1 ugiL U 1 ug/L OK TW4-26 Nitrate+Nitrite as N 1 ugiL D 0.1 ug/L OK TW4-27 Chloride 5 mg/L D 1 mg/L OK TW4-27 Carbon tetrachloride 1 ugiL U 1 ug/L OK TW4-27 Chloroform 1 ugiL U 1 ug/L OK TW4-27 Chloromethane 1 ug/L U 1 ug/L OK TW4-27 Methylene chloride 1 ug/L U 1 ugiL OK TW4-27 Nitrate+Nitrite as N 5 ugiL D 0.1 ugiL OK TWN-60 Chloride 1 mglL U 1 mglL OK TWN-60 Carbon tetrachloride 1 ug/L U 1 ugiL OK TWN-60 Chloroform 1 ugiL 1 ug/L OK TWN-60 Chloromethane 1 ugiL U 1 ugiL OK TWN-60 Methylene chloride 1 ug/L U 1 ug/L OK TWN-60 Nitrate+Nitrite as N 0.1 ugiL U 0.1 ug/L OK MW-65 Chloride 2 mg/L D 1 mg/L OK MW-65 Carbon tetrachloride 1 ug/L U 1 ug/L OK MW-65 Chloroform 1 ug/L U 1 ug/L OK MW-65 Chloromethane 1 ug/L U 1 ug/L OK MW-65 Methylene chloride 1 ug/L U 1 ug/L OK MW-65 Nitrate+Nitrite as N 0.1 ug/L U 0.1 ug/L OK TW4-70 Chloride 2 mg/L D 1 mglL OK TW4-70 Carbon tetrachloride 1 ug/L U 1 ug/L OK TW4-70 Chloroform 1 ug/L 1 ug/L OK TW4-70 Chloromethane 1 ug/L U 1 ug/L OK TW4-70 Methylene chloride 1 ug/L U 1 ug/L OK TW4-70 Nitrate+Nitrite as N 1 ug/L D 0.1 ug/L OK 1-6 Trip Blank Evaluation Lab Report Constituent Result C12081321 Carbon tetrachloride ND ug/L Chloroform ND ug/L Chloromethane ND ug/L Methylene chloride ND ug/L C12090222 Carbon tetrachloride ND ug/L Chloroform ND ug/L Chloromethane ND ug/L Methylene chloride ND ug/L C12090481 Carbon tetrachloride ND ug/L Chloroform ND ug/L Chloromethane ND ug/L Methylene chloride ND ug/L 1-7 QAlQC Evaluation for Sample Duplicates ~, *', ; ~0n~iitu'ent c.t :~:~t'j~' ~~,lt:;"1r;;;~"~>:. 1!2" M\\'.;-3i " fMW-65 ~ ",;"%~D',(,," .{ ll';'j:c Chloride (mglL) 33 34 3 Nitrate + Nitrite (as N) ND ND NC Carbon Tetrachloride ND ND NC Chloroform ND ND NC Chloromethane ND ND NC Dichloromethane (Methylene Chloride) ND ND NC t'~"\< -Constituent:~" -", . '>;ff ;' ~tW4-25 -" TW4~ 70 '.I':?! ' °AlRP~',."C' I!'<', . '~'::' - Chloride (mgIL) 334 343 2.66 Nitrate + Nitrite (as N) 17 16 6.06 Carbon Tetrachloride ND ND NC Chloroform ND 1.3 NC Chloromethane ND ND NC Dichloromethane (Methylene Chloride) ND ND NC Per section 9.1.4 a) of the QAP sample duplicates will be considered noncompliant only when the results are greater than 5 times the required reporting limit and the RPD is greater than 20%. The sample/duplicate results are not greater than 5 times the reporting limit and as such are considered acceptable. The results are reported here for information only. 1-8 QC Control Limits for Analysis and Blanks Method Blank Detections All Method Blanks for the third quarter of2012 were non-detect. Matrix Spike % Recovery Comparison ''!: ~ , ,._-.-...---7';' .. ------,]-• ";I, ";; ',!\'ISD REC ' " ~ I , " t~hReport ' t L'~b Sample m _, ~ : .. ' Welt ,_>'1','", 'Afi~lyte _',_ :MS '%'REC ' %REC 'R;mge " ,'RPD,'" ' , C12090481 C 12090481-007 TW4-10 Carbon Tetrachloride 140 144 70-130 2.5 C12090481 C 12090481-007 TW4-10 Chloroform 129 132 70-130 1.8 C12090481 C 12090481-007 TW4-10 Methylene Chloride 127 135 70-130 6.4 C12090481 C 12090481-007 TW4-10 Carbon Tetrachloride 144 144 70-130 0.6 C12090481 C 12090481-007 TW4-10 Chloroform 139 140 70-130 0.6 C12090481 C 12090481-007 TW4-10 Chloromethane 96 120 70-130 22 C12090481 C12090632-004 N/A Chloromethane 142 136 70-130 4.6 C12090481 C12090481-015 N/A Chloromethane 152 134 70-130 12 C12090222 C 12090222-007 TW4-65 Carbon Tetrachloride 143 145 70-130 1.1 C12090222 C 12090222-007 TW4-65 Chloroform 12 -4 70-130 10 C12090222 C 12090222-007 TW4-65 Carbon Tetrachloride 138 131 70-130 5.6 C12090222 C 12090222-007 TW4-65 Chloromethane 167 145 70-130 14 C12081321 CI2081321-008 TW4-09 Chloromethane 133 140 70-130 5.3 C12081321 C 12090 159-006 N/A Carbon Tetrachloride 140 135 70-130 3.5 C12081321 C12090159-006 N/A Chloromethane 132 127 70-130 3.7 NA -Not an EFR sample Laboratory Control Sample -",", , " -,'; , { , , .' .. -". .;.: -QAP-, ~ , ,f I • ilI';.. ~ " ~ '!I " ;1 '''~ .-I:i Lab Specine~ RE'C .. ,,' ' ~.;j Required , r-'!, Ii >~ , ': lj~l? Report ,--~A,nalyte LCS %RE~. R~lnge Raoge C12090481 Carbon Tetrachloride 142 70-130 None C12090481 Chloroform 134 70-130 None C12090481 Chloromethane 147 70-130 None C12090222 Chloromethane 140 70-130 None C12081321 Chloromethane 155 70-130 None 1-8 QC Control Limits for Analysis and Blanks Surrogate % Recovery C12090481 TW4-25R C12090481 TW4-25 C12090481 TW4-25 C12090481 TW4-26 C12090481 TW4-26 C12090481 TW4-06 . C12090481 TW4-06 C12090481 TW4-05 C12090481 TW4-05 C12090481 TW4-10 C12090481 TW4-10 C12090481 TW4-70 C12090481 TW4-70 C12090481 TW4-70 C12090481 LCS (9/22) C12090481 LCS (9/22) C12090481 Method Blank (9/22) C12090481 Method Blank (9/22) C12090481 Method Blank (9/22) C12090481 Matrix Spike (9/22) C12090481 Matrix Spike (9/22) C12090481 Matrix Spike (9/22) C12090481 Matrix Spike Duplicate (9/22) C12090481 Matrix Spike Duplicate (9/22) C12090481 Matrix Spike Duplicate (9/22) C12090481 Method Blank (9/23) C12090481 Matrix Spike (9/24) C12090481 Matrix Spike Duplicate (9/24) C12090222 TW4-19 C12090222 TW4-19 C12090222 TW4-19 C12090222 MW-32 C12090222 MW-32 C12090222 MW-32 C12090222 MW-04 C12090222 MW-04 . ~ . L~~f~~':O: j!'~~A"~;: M i, .'Spe·~It1e~, ~.:Requ!~ed : ~ :MCJ.t~'ng:e: ~ ~~n_ng~_ p-Bromofluorobenzene 128 80-120 None p-Bromofluorobenzene I 129 80-120 None Dibromofluoromethane 136 70-130 None p-Bromofluorobenzene 132 80-120 None Dibromofluoromethane 138 70-130 None p-Bromofluorobenzene 129 80-120 None Dibromofluoromethane 138 70-130 None p-Bromofluoro benzene 130 80-120 None Dibromofluoromethane 138 70-130 None p-Bromofluorobenzene 130 80-120 None Dibromofluoromethane 143 70-130 None p-Bromofluorobenzene 137 80-120 None Dibromofluoromethane 159 70-130 None Tolune-d8 126 80-120 None Dibromofluoromethane 139 70-130 None Tolune-d8 128 80-120 None p-Bromofluorobenzene 133 80-120 None Dibromofluoromethane 132 70-130 None Tolune-d8 125 80-120 None p-Bromofluorobenzene 126 80-120 None Dibromofluoromethane 148 70-130 None Tolune-d8 131 80-120 None p-Bromofluorobenzene 125 80-120 None Dibromofluoromethane 146 70-130 None Tolune-d8 129 80-120 None p-Bromofluorobenzene 128 80-120 None Dibromofluoromethane 132 70-130 None Dibromofluoromethane 135 70-130 None Dibromofluoromethane 146 70-130 None p-Bromofluorobenzene 138 80-120 None Tolune-d8 127 80-120 None Dibromofluoromethane 157 70-130 None p-Bromofluorobenzene 138 80-120 None Tolune-d8 128 80-120 None Dibromofluoromethane 148 70-130 None p-Bromofluorobenzene 140 80-120 None 1-8 QC Control Limits for Analysis and Blanks i;I;IY~!~~':' ~', '~' $~r )if"-,"'" ,."~;.< 'II)"""" 141~~' '.'; "".' ? ". ,:7,"~'~.~;t:, I'"J!?, "i."",,,,,,,,,;,, '. ii"!' ~, _Of_,~i' ,';; """i,. %' .~., I~ 'j':, !; '~':t . '; ~"§~;~~e~'-": ,,'<QA.~ ';: ,,~ ~:ii : ~fteq~li:~di , ~'~~:~~~D ~~~~tt ,~·:~, 'i« .,. ,.-;f,,' ;.,.-,[,1 •• wi.,<,< "'~i , i ,') '~< f_ .' ',,~ :~~Dai~Y.te;,:. = ' ~" ; Sq:rf9gate: ~~Et , ,: kE~Rp,;ngei '" -,' ,- ,~,w ':'~\:'",,: '"" R~J!g~' , C12090222 MW-04 Tolune-d8 129 80-120 None C12090222 TW4-04 Dibromofluoromethane 161 70-130 None C12090222 TW4-04 p-Bromofluorobenzene 140 80-120 None C12090222 TW4-04 Tolune-d8 129 80-120 None C12090222 MW-26 Dibromofluoromethane 151 70-130 None C12090222 MW-26 p-Bromofluorobenzene 137 80-120 None C12090222 MW-26 Tolune-d8 129 80-120 None C12090222 TW4-20 Dibromofluoromethane 137 70-130 None C12090222 TW4-20 p-Bromofluorobenzene 142 80-120 None C12090222 TW4-20 Tolune-d8 138 80-120 None C12090222 TW4-65 Dibromofluoromethane 136 70-130 None C12090222 TW4-65 p-Bromofluorobenzene 141 80-120 None C12090222 TW4-65 Tolune-d8 125 80-120 None C12090222 Trip Blank 6746 Dibromofluoromethane 136 70-130 None C12090222 Trip Blank 6746 p-Bromofluorobenzene 137 80-120 None C12090222 Trip Blank 6746 Tolune-d8 126 80-120 None C12090222 LCS (9/11) Tolune-d8 129 80-120 None C12090222 Method Blank (9/11) p-Bromofluorobenzene 137 80-120 None C12090222 Method Blank (9/11) Tolune-d8 124 80-120 None C12090222 Matrix Spike (9/11) Dibromofluoromethane 150 70-130 None C12090222 Matrix Spike (9/11) p-Bromofluorobenzene 127 80-120 None C12090222 Matrix Spike (9/11) Tolune-d8 133 80-120 None C12090222 Matrix Spike Duplicate (9/11) Dibromofluoromethane 148 70-130 None C12090222 Matrix Spike Duplicate (9/11) p-Bromofluorobenzene 126 80-120 None C12090222 Matrix Spike Duplicate (9/11) Tolune-d8 131 80-120 None C12090222 LCS (9/12) Tolune-d8 126 80-120 None C12090222 Method Blank (9/12) p-Bromofluorobenzene 123 80-120 None C12090222 Method Blank (9/12) Tolune-d8 122 80-120 None C12090222 Matrix Spike (9/12) p-Bromofluorobenzene 126 80-120 None C12090222 Matrix Spike (9/12) Tolune-d8 125 80-120 None C12090222 Matrix Spike Duplicate (9/12) p-Bromofluorobenzene 125 80-120 None C12090222 Matrix Spike Duplicate (9/12) Tolune-d8 126 80-120 None C12090222 LCS (9/13) Tolune-d8 129 80-120 None C12090222 Method Blank (9/13) p-Bromofluorobenzene 135 80-120 None C12090222 Method Blank (9/13) Tolune-d8 124 80-120 None C12090222 Matrix Spike (9/13) Dibromofluoromethane 132 70-130 None C12090222 Matrix Spike (9/13) p-Bromofluorobenzene 127 80-120 None 1-8 QC Control Limits for Analysis and Blanks C12090222 Matrix Spike (9/13) C12090222 Matrix Spike Duplicate (9/13) C12090222 Matrix Spike Duplicate (9/13) C12090222 Matrix Spike Duplicate (9/13) C12090222 LCS (9/14) C12090222 Method Blank (9/14) C12090222 Method Blank (9/14) C12090222 Method Blank (9/14) C12090222 Matrix Spike (9/14) C12090222 Matrix Spike (9/14) C12090222 Matrix Spike Duplicate (9/14) C12090222 Matrix Spike Duplicate (9/14) C12081321 TW4-03R C12081321 TW4-03 C12081321 TW4-12 C12081321 TW4-13 C12081321 TW4-14 C12081321 TW4-23 C12081321 TW4-08 C12081321 TW4-09 C12081321 TW4-16 C12081321 TW4-16 C12081321 Method Blank (9/4) C12081321 Matrix Spike (9/4) C12081321 Matrix Spike Duplicate (9/4) C12081321 Matrix Spike (9/4) C12081321 LCS (9/7) C12081321 Method Blank (9/7) C12081321 Matrix Spike (9/7) C12081321 Matrix Spike Duplicate (9/7) #II3lyti 2':To ", •... ," ' ,;S9tt'big~'te,S~~9:{i;t~, ' Tolune-d8 130 Dibromofluoromethane 137 p-Bromofluorobenzene 128 Tolune-d8 128 Tolune-d8 132 Dibromofluoromethane 132 p-Bromofluorobenzene 134 Tolune-d8 125 p-Bromofluoro benzene 123 Tolune-d8 130 p-Bromofluorobenzene 122 Tolune-d8 129 p-Bromofluoro benzene 126 p-Bromofluorobenzene 126 p-Bromofluorobenzene 125 p-Bromofluorobenzene 129 p-Bromofluorobenzene 126 p-Bromofluorobenzene 128 p-Bromofluorobenzene 126 p-Bromofluorobenzene 124 Dibromofluoromethane 133 p-Bromofluorobenzene 128 p-Bromofluorobenzene 126 Tolune-d8 124 Tolune-d8 122 p-Bromofluorobenzene 79 Tolune-d8 121 p-Bromofluorobenzene 125 Tolune-d8 124 Tolune-d8 123 ~<r~;i'-;i .. =' l:J~b"'~:':!~AP' ~i , S;D,ed{l'ed ' Req.~ir:edl " 'll~~~:'R~ngl~,: ,B~nge 80-120 I None 70-130 I None 80-120 I None 80-120 I None 80-120 I None 70-130 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 70-130 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 80-120 None 1-9 Rinsate Evaluation All rinsate samples were non-detect for the third quarter of2012. TabJ Kriged Current Quarter Chloroform Isoconcentration Map NS = not sampled; ND = not detected "-7, chloroform isocon and label MW-4 h d .. II h . • 1500 perc e m?nit?nng we sowing concentration In ug/L TW4-1 0 1000 temp?rary perched .mo~itoring well showing concentration In ug/L TWN-1 ~NS PIEZ-1 ~ NS TW4-27 ~ND temporary perched nitrate monitoring well (not sampled) perched piezometer (not sampled) temporary perched monitoring well installed October, 2011 showing concentration in ug/L HYDRO GEO CHEM, INC. KRIGED 3rd QUARTER, 2012 CHLOROFORM (ug/L) WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H:i718000/nov12/UchI0912.srf J-1 TabK Analyte Concentrations Over Time 2000 1.4 <1 <1 5.3 14-Dec-09 1800 1.6 ND ND 5.8 44 17-Feb-l0 1600 1.2 ND ND 4 45 14-Jun-l0 2100 1.2 ND ND 5.1 41 16-Aug-l0 1900 1.5 ND ND 4.8 38 11-0ct-l0 1500 1.4 ND ND 4.9 41 23-Feb-ll 1700 1.5 ND ND 4.6 40 I-Jun-ll 1700 1.4 ND ND 4.9 35 17-Aug-ll 1700 1.1 ND ND 4.9 41 16-Nov-ll 1600 1.3 ND ND 5.1 40 23-Jan-12 1500 ND ND 4.8 41 6-Jun-12 1400 1.2 ND ND 4.9 39 4-Sep-12 1500 1.5 ND ND 5 41 . . ·~·;lr/~· ..~ q,$:' .... t~~Jr ·tI-·-~, · -"~ "'h",." I~: " .' ,'1 I~f' 'C'hi : "t:, ~a~.bg I t Met,hylene ;, if' €bJior,i(l~~ Ifj~ , . . (!)'I'Q " , 1 Ol'(i)me '. I~ l'W4-1 '.' (. 11) . 'fetracbJor .' (11)' Chloride : (IIi~ '(mgM) ,: I' . ':' : ug ',~ " " ug .~, .' I', ru f :e£~ ."-1~.' ~,~ .!F!\.'IoIf ;'", (ug/l) ,],)" A~ To " .,,'~:'~ (ugfl) . i", Iii 28-Jun-99 1700 7.2 10-Nov-99 5.8 15-Mar-00 1100 10-Apr-00 1490 6-Jun-00 1530 2-Sep-00 2320 5.58 30-Nov-00 3440 7.79 29-Mar-Ol 2340 7.15 22-Jun-Ol 6000 8.81 20-Sep-Ol 12.8 8-Nov-Ol 3200 12.4 26-Mar-02 3200 13.1 22-May-02 2800 12.7 12-Sep-02 3300 12.8 24-Nov-02 3500 13.6 28-Mar-03 3000 12.4 23-Jun-03 3600 12.5 12-Sep-03 2700 12.5 8-Nov-03 3400 11.8 29-Mar-04 3200 11 22-Jun-04 3100 8.78 17-Sep-04 2800 10.8 17-Nov-04 3000 11.1 16-Mar-05 2700 9.1 25-May-05 3080 NA NA NA 10.6 NA 31-Aug-05 2900 <10 <10 <10 9.8 NA I-Dec-05 2400 <50 <50 <50 9.7 NA 9-Mar-06 2700 <50 <50 <50 9.4 49 14-Jun-06 2200 <50 <50 <50 9.8 48 20-Jul-06 2840 <50 <50 <50 9.7 51 8-Nov-06 2260 1.4 <1 <1 9.4 47 28-Feb-07 1900 1.2 <1 <1 8.9 47 27-Jun-07 1900 1.4 <1 <1 9 45 15-Aug-07 2300 1.3 <1 <1 8.4 43 10-0ct-07 2000 1.3 <1 <1 7.8 43 26-Mar-08 2000 1.3 <1 <1 7.6 39 25-Jun-08 1900 1.1 <1 <1 8.68 39 10-Sep-08 1700 1.3 <1 <1 8.15 35 15-0ct-08 1700 1.3 <1 <1 9.3 41 I,Hi", ' ,W,,"'Z,#i, ,:.\ , ~1i, .iIl, ::If, ,,'~~" ~".':i{'i' \;~f" IF ,"~ ~f '~ '~~ 1~!"Jil, m!1', ',~ ',~, ',,' I~~'$l' ~, TW4-1 ,:~i: ;fC'llloroJolC~, '" If' I ~ .ua'rb(i)D :: ~~IiI~r!lmedi'",!~. I~ Methy.;leo,e4& I:: N.~C ',.~.(i T ' hi.,'" I\\'~, Clllo~ide ~, I~ l ,ra1te' IIIfi e ;,:~, (ugJ1) et .. a~ ,O~I , e ' (mg/l) ,ii' 'f' I~ :.~ (ug/l) <,r~ ,: (llgll) , ,t ' (Ug1~!t ' (mg/l) Jill, It,',', :: '\" ,,' _ ~ 'r _ ~ '~i;'{! • II-Mar-09 1700 1.1 <1 <1 7.5 37 24-Jun-09 1500 1 <1 <1 6.9 37 15-Sep-09 1700 <1 <1 <1 7.3 36 29-Dec-09 1400 <1 <1 <1 6.8 41 3-Mar-l0 1300 <1 <1 <1 7.1 35 15-Jun-l0 1600 1.2 <1 <1 6.8 40 24-Aug-l0 1500 <1 <1 <1 6.8 35 14-0ct-l0 1500 <1 <1 <1 6.6 40 24-Feb-ll 1300 ND ND ND 6.6 41 I-Jun-ll 1200 ND ND ND 7 35 18-Aug-ll 1300 ND ND ND 6.8 36 29-Nov-ll 1300 ND ND ND 6.6 37 19-Jan-12 1300 ND ND ND 6.8 38 14-Jun-12 1000 ND ND ND 7.1 42 13-Sep-12 1000 ND ND ND 5 39 2.6 <1 <1 6.7 43 3300 2.5 <1 <1 6.6 43 14-0ct-l0 3000 2.l <1 <1 6.5 41 24-Feb-ll 3100 2.4 ND ND 7 46 2-Jun-ll 3000 2.2 ND ND 6.8 42 17-Aug-ll 2400 1.6 ND ND 6 48 29-Nov-ll 3900 2.8 ND ND 7 49 24-Jan-12 2500 2 ND ND 7.1 49 14-Jun-12 2500 2.1 ND ND 7.7 52 13-Sep-12 2900 1.8 ND ND 4 76 ~'" ' ~'~ > "Ctrb ," ;:£~. , ','iii; ":1!!. '~ ': .. ;~ ~. ~~i~~ 'j., ~ '~i . ;;~ €1iI~!!4:!~ i:i-etrachl ~ 'CbIQ'rome*b tll~lenel I !i~·: '€' ~' f'{e , ride~ .~ "~DA-J } . (ugll) . Itloride"~ 4: .'''4 (mgll). '", :i"".\.. . I"~~ {uell} " "~ , , ; .. ri(ue/I:) ".'lJ{'!',! ',. '.o,F::.. ':.'i!1~ f'I ",,' '~ .i. 28-Jun-99 3S00 7.6 29-Nov-99 702 IS-Mar-OO 834 2-Sep-00 836 1.S6 29-Nov-00 836 1.97 27-Mar-Ol 347 1.8S 21-Jun-Ol 390 2.61 20-Sep-Ol 300 3.06 7-Nov-Ol 170 3.6 26-Mar-02 11 3.87 21-May-02 204 4.34 12-Sep-02 203 4.32 24-Nov-02 102 4.9 28-Mar-03 0 4.6 23-Jun-03 0 4.8 12-Sep-03 0 4.3 8-Nov-03 0 4.8 29-Mar-04 0 4.48 22-Jun-04 0 3.68 17-Sep-04 0 3.88 17-Nov-04 0 4.1 16-Mar-OS 0 3.S 2S-May-OS <1 NA NA NA 3.7 NA 31-Aug-OS <1 <1 6.4 <1 3.S NA I-Dec-OS <1 <1 2.3 <1 3.3 NA 9-Mar-06 <1 <1 2.2 <1 3.3 26 14-Jun-06 <1 <1 <1 <1 3.2 26 20-Jul-06 <1 <1 1.6 <1 2.9 26 8-Nov-06 <I <1 <1 <1 1.S 23 28-Feb-07 <1 <1 <1 <1 3.1 22 27-Jun-07 <1 <1 <1 <1 3.3 23 IS-Aug-07 <1 <1 <1 <1 3.1 24 10-0ct-07 <1 <1 <1 <1 2.8 27 26-Mar-08 <1 <1 <1 <1 2.8 21 2S-Jun-08 <1 <1 <1 <1 2.8S 19 10-Sep-08 <1 <1 <1 <1 2.66 19 IS-0ct-08 <1 <1 <1 <1 2.63 22 4-Mar-09 <1 <1 <1 <1 2.S 21 24-Jun-09 <1 <1 <1 <1 2.9 20 ·'~;,f:'-;/'.' 1'1'(;;' :'ii.' , ."'" 'l!-. ,,".: 4~'~·O!l:iil~ .. ~... .. ~ .. I~ M~ib~tin~~" Nit~atle .~~ , .~~~ r" 1'W4-3 :, 'I ;i~~Cbl'O'r0fhrm l' 'fit-T . bl .. €lilQ'FOmethane,; C~19ride' ~i • , orl e~ 1& .' u fI ,II I~Chlolri(le ~ ~ (mgJ1~ • .y-. = ,Ji, . -_ (ugn) '. if'~::-(U2~l .';~" I.. 'j' (g) " ." {u2f11 ' ' (mglI~ .:". p ~. .." ,,, 15-Sep-09 <1 <1 <1 <1 2.8 21 16-Dec-09 <1 <1 <1 <1 2.5 22 23-Feb-10 <1 <1 <1 <1 2.8 23 8-Jun-10 <1 <1 <1 <1 3 24 10-Aug~10 <1 <1 <1 <1 3.1 22 5-0ct-10 <1 <1 <1 <1 3.3 26 15-Feb-11 ND ND ND ND 3.5 23 25-May-11 ND ND ND ND 3.7 23 16-Aug-11 ND ND ND ND 4 23 15-Nov-11 ND ND ND ND 4.4 23 17-Jan-12 ND ND ND ND 4.3 21 31-May-12 ND ND ND ND 4.4 24 29-Aug-12 ND ND ND ND 4.9 25 w ,~~~~~~/~~~,-carbon~l;' ",':" ¢ ~.ethYlene~'~ ',$ ',~ ~ I'!" C'ltl ' ,,' ' 'el11 " tli P-< ~~~~ , ~€1I1 "d ' ' j;Ir'?! ' , c or ~ 1Tetr.ac·hJo~i :, ,orQRl.e ane ~? ~lilnFide"~ ,;, " , , ~n " e,;. I'\!. , " 'r!., ~u '~. . ' , ' ~ugll) , ,~ ~" " , . . v, '~ (~g7l~ IIh ,(~ ~mgM)~:'l'~: .~ <" ~ "" ,.!t; ';~~:';\i ~,~'\\.o .,,;r~ r~·(rU~(:J.)'1' ".." " "".0 J ~, ,~,(U:21:1} , "c"" ,';;1 ".,. ~ 'ii, 6-Jun-00 0 2-Sep-00 0 28-Nov-00 3.9 28-Mar-01 2260 1.02 20-Jun-01 3100 14.5 20-Sep-01 3200 14 8-Nov-01 2900 14.8 26-Mar-02 3400 15 22-May-02 3200 13.2 12-Sep-02 4000 13.4 24-Nov-02 3800 12.6 28-Mar-03 3300 13.4 23-Jun-03 3600 12.8 12-Sep-03 2900 12.3 8-Nov-03 3500 12.3 29-Mar-04 3200 12.2 22-Jun-04 3500 12.1 17-Sep-04 3100 11.1 17-Nov-04 3600 10.8 16-Mar-05 3100 11.6 25-May-05 2400 NA NA NA 11.3 NA 31-Aug-05 3200 <10 <10 <10 9.9 NA I-Dee-05 2800 <50 <50 <50 10.2 NA 9-Mar-06 2900 <50 <50 <50 9.5 51 14-Jun-06 2600 <50 <50 <50 8.6 48 20-Jul-06 2850 <50 <50 <50 9.7 50 8-Nov-06 2670 1.7 <1 <1 10.1 49 28-Feb-07 2200 1.5 <1 <1 9 49 27-Jun-07 2400 1.7 <1 <1 9.4 47 15-Aug-07 2700 1.5 <1 <1 9.5 45 10-0et-07 2500 1.5 <1 <1 9.5 47 26-Mar-08 2800 1.6 <1 <1 9.2 43 25-Jun-08 2500 1.5 <1 <1 10.8 42 10-Sep-08 2200 1.4 <1 <1 8.83 39 15-0et-08 2500 2 <2 <2 10.1 44 4-Mar-09 2200 1.2 <1 <1 10.2 37 24-Jun-09 1800 1.2 <1 <1 8.2 34 15-Sep-09 2000 1.1 <1 <1 8.4 39 29-Dee-09 950 1.1 <1 <1 7.6 41 10-Jun-l0 2000 1.2 <1 <1 7.6 35 16-Aug-l0 2100 1.3 <1 <1 7.3 36 11-0ct-l0 1700 1.3 <1 <1 7.1 38 23-Feb-ll 1800 1.4 ND ND 7 41 I-Jun-ll 1700 1.2 ND ND 7 35 17-Aug-ll 1500 ND ND ND 6.6 40 16-Nov-ll 1500 1 ND ND 7 39 23-Jan-12 1200 ND ND ND 7.1 38 6-Jun-12 1500 ND ND ND 7.1 43 4-Sep-12 1600 1.2 ND ND 7.1 39 ~'f"", . '/);.,". Carboi'i ~ -," _tbYh:ne O"'I~~~;;ii'i , ~ChIDvoform' :~t;' ., I(j)Fomef . ~ ovUle" . -. (u~;' _ ' Tetrachlorule., (ugJl) . ;,: bhlllliJe ".;: ( " ~ ;mgtI) .f .1 ,.,: ," ." ,Z, ,~: f,; ~ .~ '~U2I1Y ",\~' ,"IIi; ·,,1, I!' :Of; "~1ti'2f1)i; r _"-}~~ .,' . ~_, Ji! 20-Dee-99 29.5 15-Mar-00 49.0 2-Sep-00 124 29-Nov-00 255 28-Mar-Ol 236 20-Jun-Ol 240 20-Sep-Ol 240 7-Nov-Ol 260 26-Mar-02 260 22-May-02 300 12-Sep-02 330 24-Nov-02 260 28-Mar-03 240 23-Jun-03 290 12-Sep-03 200 8-Nov-03 240 29-Mar-04 210 22-Jun-04 200 17-Sep-04 150 17-Nov-04 180 16-Mar-05 120 25-May-05 113 NA NA NA 3.7 NA 31-Aug-05 82.0 <2.5 5.8 <2.5 6 NA I-Dee-05 63.0 <2.5 2.5 <2.5 6 NA 9-Mar-06 66.0 <2.5 3.1 <2.5 6 52 14-Jun-06 51.0 <1 <2.5 <2.5 5.9 51 20-Jul-06 53.7 <1 <1 <1 6.7 54 8-Nov-06 47.1 <1 <1 <1 2.9 55 28-Feb-07 33.0 <1 <1 <1 7.8 57 27-Jun-07 26.0 <1 <1 <1 7 45 15-Aug-07 9.2 <1 <1 <1 7.7 38 10-0et-07 9.4 <1 <1 <1 8.2 39 26-Mar-08 11.0 <1 <1 <1 7.4 36 25-Jun-08 9.3 <1 <1 <1 8.7 37 10-Sep-08 11.0 <1 <1 <1 7.91 34 15-0et-08 10.0 <1 <1 <1 9.3 37 4-Mar-09 12.0 <1 <1 <1 7.9 34 24-Jun-09 13.0 <1 <1 <1 7.5 37 15-Sep-09 12.0 <1 <1 <1 8.3 48 13.0 <1 <1 <1 6.8 43 9-Jun-10 12.0 <1 <1 <1 7.1 28 11-Aug-10 12.0 <1 <1 <1 7 38 13-0ct-10 11.0 <1 <1 <1 7.2 41 22-Feb-11 10.0 ND ND ND 7 34 26-May-11 9.0 ND ND ND 7.2 35 17-Aug-11 10.0 ND ND ND 7.5 37 7-Dec-11 7.9 ND ND ND 6 30 18-Jan-12 7.6 ND ND ND 5.8 22 6-Jun-12 8.4 ND ND ND 8 39 11-Sep-12 12.0 ND ND ND 8.1 37 ~., ~ '~~f -~l~bon If~~' ·~f;fieen. '[II e -6 "" , CId~Fol! • i't ~ 'hI , "d ,otomothane .".." I~it., ,itte' . . (fl . e Fae • 0Fl . r 11) rl e ~: lit! ' < ~l~ . ug frii {u l~~" I ug It m g ,(~,I' ~, "'l.~",~' Vl,,' , '~o" tig/l ,!I~'ic", 'l', ;ill "'"1Il '~,~1 ...;I~ .~ y ~' 6-Jun-00 0 2-Sep-00 0 28-Nov-00 0 ND 26-Mar-OI 0 0.13 20-Jun-OI 0 ND 20-Sep-OI 4 ND 7-Nov-OI 1 ND 26-Mar-02 0 ND 2I-May-02 0 ND 12-Sep-02 0 ND 24-Nov-02 0 ND 28-Mar-03 0 0.1 23-Jun-03 0 ND 12-Sep-03 0 ND 8-Nov-03 0 ND 29-Mar-04 0 ND 22-Jun-04 0 ND 17-Sep-04 0 ND 17-Nov-04 0 ND 16-Mar-05 0 0.2 25-May-05 2.5 NA NA NA 0.4 NA 3I-Aug-05 10.0 <1 2.8 <1 0.8 NA I-Dec-05 17.0 <1 1.3 <1 0.9 NA 9-Mar-06 31.0 <1 <1 <1 1.2 31 14-Jun-06 19.0 <1 <1 <1 1 30 20-Jul-06 11.0 <1 <1 <1 0.6 37 8-Nov-06 42.8 <1 <1 <1 1.4 65 28-Feb-07 46.0 <1 <1 <1 1.5 32 27-Jun-07 11.0 <1 <1 <1 0.6 38 15-Aug-07 18.0 <1 <1 <1 0.7 36 IO-Oct-07 18.0 <1 <1 <1 0.8 38 26-Mar-08 52.0 <1 <1 <1 1.1 33 25-Jun-08 24.0 <1 <1 <1 0.9 35 IO-Sep-08 39.0 <1 <1 <1 1.14 35 15-0ct-08 37.0 <1 <1 <1 1.01 33 II-Mar-09 81.0 <1 <1 <1 2.2 35 24-Jun-09 120 <1 <1 <1 2.7 37 15-Sep-09 280 <1 <1 <1 5.0 37 22-Dec-09 250 <1 <1 <1 6.1 41 25-Feb-IO 1000 <1 <1 <1 1.6 45 IO-Jun-IO 590 <1 <1 <1 2.5 33 12-Aug-IO 630 <1 <1 <1 3.9 31 13-0ct-IO 420 <1 <1 <1 4.3 41 23-Feb-II 47 ND ND ND 0.7 40 17-Aug-11 16 39 7-Dec-ll 21 ND ND ND 0.8 36 18-Jan-12 38 ND ND ND 0.7 38 13-Jun-12 4.7 ND ND ND 0.2 40 11-Sep-12 6.9 ND ND ND O.l 21 15-Mar-00 616 2-Sep-00 698 29-Nov-00 684 1.99 28-Mar-Ol 747 2.46 20-Jun-Ol 1100 2.65 20-Sep-Ol 1200 3.38 8-Nov-Ol . 1100 2.5 26-Mar-02 1500 3.76 23-May-02 1600 3.89 12-Sep-02 1500 3.18 24-Nov-02 2300 4.6 28-Mar-03 1800 4.8 23-Jun-03 5200 7.6 12-Sep-03 3600 7.6 8-Nov-03 4500 7.1 29-Mar-04 2500 4.63 22-Jun-04 2900 4.83 17-Sep-04 3100 5.59 17-Nov-04 3800 6 16-Mar-05 3100 5.2 25-May-05 2700 NA NA NA 5.4 NA 31-Aug-05 3100 <10 <10 <10 5.2 NA I-Dec-05 2500 <50 <50 <50 5.3 NA 9-Mar-06 1900 <50 <50 <50 1 48 14-Jun-06 2200 <50 <50 <50 4.5 47 20-Jul-06 2140 <50 <50 <50 4.7 51 8-Nov-06 2160 1.5 <1 <1 4.6 49 28-Feb-07 1800 1.1 <1 <1 5 47 27-Jun-07 2600 1.5 <1 <1 5.1 45 14-Aug-07 2300 1.4 <1 <1 4.7 44 10-0ct-07 1900 1.2 <1 <1 4.7 45 26-Mar-08 2200 1.3 <1 <1 4.2 43 25-Jun-08 1800 1.3 <1 <1 4.8 43 10-Sep-08 1600 1.4 <1 <1 4.16 35 15-0ct-08 1900 <2 <2 <2 4.01 40 II-Mar-09 1800 1.2 <1 <1 3.7 35 24-Jun-09 1400 <1 <1 <1 3.8 37 15-Sep-09 1500 1.0 <1 <1 4.1 37 , ~'~'. ~f:f~r .'>i' . · ~1f/J' "~i=' .. r:~~~:~~;; ~~cbi:lid~:. !.m ~ ..., l(i)r6f0JEm~\' >4j ., Fbon .' 'f", .. '. ." 1';C , "'ifW4-7 ,' . ' if . ,;; Tet . . 1l16ri4~ Clllo~ ,e1ba:ne. . . . I:r·" (ugfl) ;~ . u II, _ i!1 I, -, mg: ' -(mgfl} ~ % " Ii _ ~. 'rI! >~cJ ~(lt2/n , 'til( \if . -'. ..;' -' ·(~2!.l) . '. ; 29-Dec-09 1300 <1 <1 <1 4.2 37 3-Mar-10 1200 <1 <1 <1 3.8 36 1 0-Jun-1 0 1100 <1 <1 <1 3.9 31 18-Aug-10 1500 1.1 <1 <1 3.9 36 13-0ct-10 1100 1.1 <1 <1 4 38 23-Feb-11 1300 ND ND ND 3.6 45 1-Jun-11 1200 ND ND ND 4 35 18-Aug-11 1200 ND ND ND 4.1 37 29-Nov-11 1000 ND ND ND 3.8 37 19-Jan-12 1000 ND ND ND 3.9 37 14-Jun-12 790 ND ND ND 4 41 13-Sep-12 870 ND ND ND 3.8 40 ~I': .c"r.B~Ylene:'.II_ elll , " • ro.m, '. ~# I~f; OF . -k.l. (~~trwch'10n ( 'Ai) " ol1'lile ~:."~ . (l' . Ik ',' m.l~#''''~ ",;..Ji'i'. I ;"t1,. • "., ug ,. . . , 1';~lIlj , m:g . .ii' ~_~_':~ -';"""\"". . ~. ;. 1~,'t'''21l'! .,_" ,,,, .!., '>1 '"[f~ 0211), Ill] -'I>. ~ It\}'~ -,' i~ 29-Nov-99 0 IS-Mar-OO 21.8 2-Sep-00 102 29-Nov-00 107 ND 26-Mar-Ol 116 ND 20-Jun-Ol 180 ND 20-Sep-Ol 180 0.3S 7-Nov-Ol 180 ND 26-Mar-02 190 0.62 22-May-02 210 0.77 12-Sep-02 300 ND 24-Nov-02 4S0 ND 28-Mar-03 320 0.8 23-Jun-03 420 ND 12-Sep-03 66.0 ND 8-Nov-03 21.0 0.1 29-Mar-04 24.0 0.6S 22-Jun-04 110 0.S2 17-Sep-04 120 ND 17-Nov-04 120 ND 16-Mar-OS 10.0 ND 2S-May-OS <1 NA NA NA 0.2 NA 31-Aug-OS 1.1 <1 1.7 <1 <0.1 NA 30-Nov-OS <1 <1 <1 <1 <0.1 NA 9-Mar-06 1.3 <1 2.1 <1 0.3 39 14-Jun-06 1.0 <1 1.8 <1 <0.1 37 20-Jul-06 <1 <1 <1 <1 0.1 39 8-Nov-06 <1 <1 <1 <1 <0.1 40 28-Feb-07 2.S <1 <1 <1 0.7 39 27-Jun-07 2.S <1 <1 <1 0.2 42 IS-Aug-07 1.S <1 <1 <1 <0.1 42 10-0ct-07 3.S <1 <1 <1 O.S 43 26-Mar-08 <1 <1 <1 <1 0.1 46 2S-Jun-08 <1 <1 <1 <1 <O.OS 4S 10-Sep-08 <1 <1 <1 <1 <O.OS 39 IS-0ct-08 <1 <1 <1 <1 <O.OS 44 4-Mar-09 <1 <1 <1 <1 <0.1 42 24-Jun-09 <1 <1 <1 <1 <0.1 44 IS-Sep-09 <1 <1 <1 <1 <1 44 i~; '," "~Jf''''~ < ~i ~arb ' ".--'" . !;l~~'~ ·byle.ne t1iii . i:Jti'J~~ r,ll .10 .'fi;l{ Glllo»" , 0FomeUli Ghhnide ,~ C;hl ~' :retrach'lo~ (ugn) (m~~f: ' (u ,fiJ" i. (1!~) '''' 1 "'i (n~:l ~m~) -' .'~ ",!!! .,""", iX 3>~"', ."" .,~, JI ',," .",_ !'I 21-Jan-02 14 26-Mar-02 16 0.14 21-May-02 17 0.11 12-Sep-02 6 ND 24-Nov-02 14 ND 28-Mar-03 29 0.2 23-Jun-03 110 0.4 12-Sep-03 74 0.4 8-Nov-03 75 0.3 29-Mar-04 22 0.1 22-Jun-04 32 ND 17-Sep-04 63 0.46 17-Nov-04 120 0.4 16-Mar-05 140 1.6 25-May-05 62.4 NA NA NA 0.8 NA 31-Aug-05 110 <2.5 6.2 <2.5 1.1 NA 1-Dec-05 300 <2.5 <2.5 <2.5 3.3 NA 9-Mar-06 190 <5 <50 <50 2.4 50 14-Jun-06 300 <5 <50 <50 3.5 54 20-Jul-06 504 <5 <50 <50 6.8 61 8-Nov-06 452 ·<1 1.6 1 5.7 58 28-Feb-07 500 <1 <1 1 7.6 62 27-Jun-07 350 <1 <1 1 5.1 54 15-Aug-07 660 <1 <1 1 7.3 59 10-0ct-07 470 <1 <1 1 6.7 59 26-Mar-08 620 <1 <1 1 7.3 55 25-Jun-08 720 <1 <1 1 9.91 58 10-Sep-08 680 <1 <1 1 9.23 51 15-0ct-08 1200 <2 <2 2 10.5 61 11-Mar-09 1100 <1 <1 1 11.6 64 24-Jun-09 1200 <1 <1 1 9.8 62 15-Sep-09 910 <1 <1 1 8.1 51 22-Dec-09 300 <1 <1 <1 3.5 51 3-Mar-10 460 <1 <1 <1 5 49 10-Jun-10 220 <1 <1 <1 1.6 42 12-Aug-10 100 <1 <1 <1 0.8 38 13-0ct-10 1100 <1 <1 <1 11 52 23-Feb-11 620 ND ND ND 9 62 1-Jun-11 280 ND ND ND 3.3 42 16-Nov-11 ND ND ND 1.1 45 19-Jan-12 76 ND ND ND 0.9 40 13-Jun-12 79 ND ND ND 0.8 46 12-Sep-12 130 ND ND ND 1.0 44 21-Jan-02 4700 26-Mar-02 4900 9.6 22-May-02 5200 9.07 12-Sep-02 6200 8.84 24-Nov-02 5800 9.7 28-Mar-03 5100 9.7 23-Jun-03 5700 9.4 12-Sep-03 4600 9.9 8-Nov-03 5200 9.3 29-Mar-04 5300 9.07 22-Jun-04 5700 8.74 17-Sep-04 4800 8.75 17-Nov-04 5800 9.7 16-Mar-05 4400 8.7 25-May-05 3590 NA NA NA 10.3 NA 31-Aug-05 4400 <10 <10 <10 9.4 NA 1-Dec-05 4400 <100 <100 <100 9.4 NA 9-Mar-06 4400 <50 <50 <50 9.2 56 14-Jun-06 4300 <50 <50 <50 10 56 20-Jul-06 4080 <50 <50 <50 10 55 8-Nov-06 3660 1.7 2.7 1.3 10 55 28-Feb-07 3500 1.3 <1 1.6 10.1 54 27-Jun-07 3800 1.6 <1 1.1 10.6 53 15-Aug-07 4500 1.7 <1 1.1 10.2 53 10-0ct-07 4400 1.6 <1 1.2 9.8 53 26-Mar-08 340 <1 <1 <1 7.7 63 25-Jun-08 640 <1 <1 <1 7.28 46 10-Sep-08 900 <1 <1 <1 7.93 42 15-0ct-08 1000 <2 <2 <2 9.46 47 11-Mar-09 1100 <1 <1 <1 7.3 49 24-Jun-09 980 <1 <1 <1 6.8 44 15-Sep-09 1000 <1 <1 <1 7 49 29-Dec-09 860 <1 <1 <1 6.6 46 3-Mar-10 820 <1 <1 <1 6.8 42 10-Jun-10 820 <1 <1 <1 6.9 40 12-Aug-10 800 <1 <1 <1 6.7 43 13-0ct-10 720 <1 <1 <1 6.4 49 23-Feb-1 L 1000 ND ND ND 6.5 46 1-Jun-11 930 ND ND ND 7.3 49 16-Nov-ll 1500 ND ND ND 7.1 24-Jan-12 610 ND ND ND 6.8 43 13-Jun-12 660 ND ND ND 6.7 52 13-Sep-12 740 ND ND ND 3 49 12-Sep-02 2 2.S4 24-Nov-02 o 2.2 28-Mar-03 o 1.9 23-Jun-03 o 1.8 12-Sep-03 o 1.8 9-Nov-03 o 1.6 29-Mar-04 o 1.S8 22-Jun-04 o 1.4 17-Sep-04 o 1.24 17-Nov-04 o 1.S 16-Mar-OS o 1.4 2S-May-OS <1 NA NA NA 1.6 NA 31-Aug-OS <1 <1 S.8 <1 1.S NA I-Dec-OS <1 <1 1.9 <2 1.4 NA 9-Mar-06 <1 <1 2.6 <1 1.3 19 14-Jun-06 <1 <1 1.4 <1 1.4 16 20-Jul-06 <1 <1 <1 <1 1.4 16 8-Nov-06 <1 <1 <1 <1 1.4 16 28-Feb-07 <1 <1 <1 <1 1.S 16 27-Jun-07 <1 <1 <1 <1 I,S 18 IS-Aug-07 <1 <1 <1 <1 1.4 29 10-0ct-07 <1 <1 <1 <1 1.4 16 26-Mar-08 <1 <1 <1 <1 1.6 16 2S-Jun-08 <1 <1 <1 <1 2.69 19 10-Sep-08 <1 <1 <1 <1 2.6S 18 IS-0ct-08 <1 <1 <1 <1 2.47 22 4-Mar-09 <1 <1 <1 <1 2.4 23 24-Jun-09 <1 <1 <1 <1 3.8 22 IS-Sep-09 <1 <1 <1 <1 S.1 22 16-Dec-09 <1 <1 <1 <1 3.6 23 23-Feb-l0 <1 <1 <1 <1 4 22 8-Jun-l0 <1 <1 <1 <1 11 29 10-Aug-l0 <1 <1 <1 <1 9 3S S-Oct-l0 <1 <1 <1 <1 8 31 IS-Feb-ll ND ND ND ND 6.S 31 2S-May-ll ND ND ND ND 7 32 16-Aug-ll ND ND ND ND 6.8 31 IS-Nov-ll ND ND ND ND 8 30 17-Jan-12 ND ND ND ND 7.7 28 ~I-~{~~r)~:];~~*~ ~t '" EE r4~~~ . 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" I2-Sep-02 ND ND 24-Nov-02 ND ND 28-Mar-03 ND 0.2 23-Jun-03 ND 0.2 I2-Sep-03 ND ND 9-Nov-03 ND 0.9 29-Mar-04 ND 0.12 22-Jun-04 ND 0.17 I7-Sep-04 ND 4.43 I7-Nov-04 ND 4.7 I6-Mar-05 ND 4.2 25-May-05 <1 NA NA NA 4.3 NA 3I-Aug-05 <1 <1 3.1 <1 4.6 NA I-Dec-05 <1 <1 <1 <1 4.3 NA 9-Mar-06 <1 <1 1.7 <1 4.2 67 I4-Jun-06 <1 <1 1.4 <1 4.9 66 20-Jul-06 <1 <1 <1 <1 4.3 65 8-Nov-06 <1 <1 <1 <1 0.8 33 28-Feb-07 <1 <1 <1 <1 4 59 27-Jun-07 <1 <1 <1 <1 4.6 59 I5-Aug-07 <1 <1 <1 <1 4.4 58 IO-Oct-07 <1 <1 <1 <1 4.1 58 26-Mar-08 <1 <1 <1 <1 3.8 54 25-Jun-08 <1 <1 <1 <1 4.24 58 IO-Sep-08 <1 <1 <1 <1 4.26 50 I5-0ct-08 <1 <1 <1 <1 4.63 58 4-Mar-09 <1 <1 <1 <1 3.7 58 24-Jun-09 <1 <1 <1 <1 1.2 57 I5-Sep-09 <1 <1 <1 <1 4.7 63 I6-Dec-09 <1 <1 <1 <1 4.1 60 24-Feb-IO <1 <1 <1 <1 4.3 53 8-Jun-IO <1 <1 <1 <1 5.2 52 1 O-Aug-I 0 <1 <1 <1 <1 5.6 55 5-0ct-IO <1 <1 <1 <1 5.8 55 I5-Feb-ll ND ND ND ND 5.5 60 25-May-II ND ND ND ND 5.4 56 I6-Aug-ll ND ND ND ND 5.2 60 I5-Nov-ll ND ND ND ND 5.9 54 I7-Jan-I2 ND ND ND ND 5.5 55 3I-May-I2 ND ND ND ND 6 59 29-Aug-I2 ND ND ND ND 6.2 60 ·~,~;,;: . . ~';:!',;'h'l:' . •• fi.· 'II' I ~ ".' ~("' il. 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",!,~,.,_ ,J u ) ."-. ,,"!I "'" • ," ."-,,, . -~' :~ ;.;10 12-Sep-02 140 ND 24-Nov-02 200 ND 28-Mar-03 260 ND 23-Jun-03 370 ND 12-Sep-03 350 ND 8-Nov-03 400 ND 29-Mar-04 430 ND 22-Jun-04 530 ND 17-Sep-04 400 ND 17-Nov-04 350 ND 16-Mar-05 240 ND 25-May-05 212 NA NA NA <0.1 NA 31-Aug-05 85 <1 3.2 43 <0.1 NA I-Dec-05 14 <2.5 2.6 5.9 1.4 NA 9-Mar-06 39.0 <1 1.1 21 3 . 60 14-Jun-06 13.0 <1 2.4 8.9 1.9 55 20-Jul-06 5.2 <1 <1 2.7 2.7 60 8-Nov-06 13.6 <1 <1 9.2 5.6 62 28-Feb-07 8.7 <1 <1 6.5 12.3 79 27-Jun-07 2.6 <1 <1 1.8 9.9 75 15-Aug-07 7.1 <1 <1 5.1 5.4 66 10-0ct-07 1.4 <1 <1 <1 4.4 69 26-Mar-08 11.0 <1 <1 26 ND 52 25-Jun-08 <1 <1 <1 <1 1.46 58 10-Sep-08 10 <1 <1 14 10.5 71 15-0ct-08 3.9 <1 <1 6.6 9.82 89 4-Mar-09 <1 <1 <1 <1 9.6 78 24-Jun-09 <1 <1 <1 <1 8.9 76 15-Sep-09 <1 <1 <1 <1 8.8 79 17-Dec-09 <1 <1 <1 <1 5.2 76 24-Feb-l0 <1 <1 <1 <1 4.2 77 9-Jun-l0 2.1 <1 <1 <1 4.7 64 24-Aug-l0 4.3 <1 <1 <1 4.6 72 6-0ct-l0 3.0 <1 <1 <1 3.3 72 22-Feb-ll 15.0 ND ND ND 7 86 26-May-ll 16.0 ND ND ND 5 81 17-Aug-ll 9.2 ND ND ND 1.7 63 16-Nov-11 ND ND ND 1.4 0.4 38 18-Jan-12 ND ND ND 1.7 0.1 48 30-Aug-12 ND ND ND ''''', 'r. '0."" ~, C'ar~Q " -~~t~~" . .-"':"~;i;, ... , ~ I;p , .' ene <2I1iIOF0£ Or(i)nu~tJfiaRe . (if ! '" I:~ Nitr . 16ri(le~ -(ug{l) 'Tetrackhu'"il ,,' " VI 'e l.'iJ ;f~ I'" (u~iO c (uwO .~ ,',] , )Jt:~:: I ~ ~m,gIll ,gil) 3i' _."', ",,>ri . ., , ., ' . It"", '",: .'!' "iJll :(0, ') l~ !j!'" ~ ,', 12-Sep-02 1.6 ND 24-Nov-02 ND ND 28-Mar-03 . ND ND 23-Jun-03 ND ND 12-Sep-03 ND ND 8-Nov-03 ND ND 29-Mar-04 ND ND 22-Jun-04 ND ND 17-Sep-04 ND ND 17-Nov-04 ND ND 16-Mar-OS ND ND 30-Mar-OS ND ND 2S-May-OS <1 NA NA NA <0.1 NA 31-Aug-OS <1 <1 3.2 <1 <0.1 NA 1-Dec-OS <1 <1 <1 <1 <0.1 NA 9-Mar-06 <1 <1 <1 <1 <0.1 32 14-Jun-06 <1 <1 3.S <1 <0.1 30 20-Jul-06 <1 <1 1.8 <1 <0.1 32 8-Nov-06 <1 <1 1.S <1 <0.1 31 28-Feb-07 <1 <1 <1 <1 <0.1 32 27-Jun-07 <1 <1 <1 <1 <0.1 32 lS-Aug-07 <1 <1 <1 <1 <0.1 31 10-0ct-07 <1 <1 <1 <1 <0.1 32 26-Mar-08 <1 <1 <1 <1 <0.1 31 2S-Jun-08 <1 <1 <1 <1 <O.OS 29 10-Sep-08 <1 <1 <1 <1 <O.OS 30 lS-0ct-08 <1 <1 <1 <1 <O.OS 26 4-Mar-09 <1 <1 <1 <1 <0.1 30 24-Jun-09 <1 <1 <1 <1 <0.1 31 lS-Sep-09 <1 <1 <1 <1 <O.l 33 16-Dec-09 <1 <1 <1 <1 <0.1 34 17-Feb-10 <1 <1 <1 <1 <0.1 38 14-Jun-10 <1 <1 <1 <1 <0.1 32 16-Aug-10 <1 <1 <1 <1 <0.1 28 6-0ct-10 <1 <1 <1 <1 <0.1 24 23-Feb-1 1 ND ND ND ND ND 40 2S-May-1 1 ND ND ND ND ND 31 16-Aug-11 ND ND ND ND ND 33 6-Dec-11 ND ND ND ND ND 32 18-Jan-12 ND ND ND ND ND 21 4-Jun-12 ND ND ND ND ND 32 5-Sep-12 ND ND ND ND ND 33 1.49 24-Nov-02 240 13.3 28-Mar-03 160 13.1 23-Jun-03 110 19 12-Sep-03 68.0 19.9 9-Nov-03 84.0 20.7 29-Mar-04 90.0 14 22-Jun-04 82.0 12.2 17-Sep-04 38.0 14.5 17-Nov-04 51.0 17.3 16-Mar-05 38.0 14.1 25-May-05 29.8 NA NA NA 12.9 NA 31-Aug-05 39 <1 2.8 <1 13.3 NA 1-Dee-05 14 <1 1.1 <1 7.3 NA 9-Mar-06 12.0 <1 1.1 <1 5.9 5.9 14-Jun-06 12.0 <1 1.6 <1 4.7 35 20-Jul-06 10.8 <1 2.7 <1 6.1 35 8-Nov-06 139 <1 <1 <1 8.7 34 28-Feb-07 9.2 <1 <1 <1 5.1 30 27-Jun-07 8.0 <1 <1 <1 4.9 28 15-Aug-07 8.9 <1 <1 <1 5 32 10-0et-07 7.4 <1 <1 <1 4.4 27 26-Mar-08 6.4 <1 <1 <1 0.7 23 25-Jun-08 5.7 <1 <1 <1 4.55 23 10-Sep-08 8.0 <1 <1 <1 4.68 26 15-0et-08 9.4 <1 <1 <1 5,15 30 4-Mar-09 11.0 <1 <1 <1 5.2 29 24-Jun-09 16.0 <1 <1 <1 6.2 30 15-Sep-09 13.0 <1 <1 <1 5.9 26 22-Dee-09 8.2 <1 <1 <1 5.4 30 24-Feb-10 69.0 <1 <1 <1 5.1 41 9-Jun-10 29.0 <1 <1 <1 9 35 12-Aug-10 29.0 <1 <1 <1 9 37 13-0et-10 30.0 <1 <1 <1 10 50 22-Feb-11 39.0 ND ND ND 10 52 26-May-11 26.0 ND ND ND 9 36 17-Aug-11 29.0 ND ND ND 4.6 23 7-Dee-11 28.0 ND ND ND 6.3 23 19-Jan-12 25.0 ND ND ND 4.4 18 ~)t ::~;: ~~; ,< .~ '. ..' '"." .. '" ~-• .' ." > !. , '. • CadJoJil, ' . ,. ,M~tti~leRe I~·.·' , '. I, TW ... CaitOI:'. l' t 1tJ .· . FODlet}ia.,~( ~Clll ' 'd ·l~ . )[m.~ I~'" . '~ . ( e rae O~I . (g7I} ,l I" (!)FI e ~. (. gnl ' ' , u ' l~: ' u l2lf: ,~m . 'ie. JI' _ I'J! (u )< !' .,,_"""-'ll . !i" ._~i!i.,,,,, to.) I" .". "''''.~" _<. '''"'. ~ 12-Sep-02 7700 47.6 24-Nov-02 5400 42 28-Mar-03 4200 61.4 15-May-03 4700 NA 23-Jun-03 4500 11.4 15-Jul-03 2400 6.8 15-Aug-03 2600 4 12-Sep-03 2500 5.7 25-Sep-03 4600 9.2 29-0ct-03 4600 7.7 9-Nov-03 2600 4.8 29-Mar-04 NA NA 22-Jun-04 NA NA 16-Aug-04 7100 9.91 17-Sep-04 2600 4.5 17-Nov-04 1800 3.6 16-Mar-05 2200 5.3 25-May-05 1200 5.7 31-Aug-05 1400 <5 <5 <5 4.6 NA 1-Dec-05 2800 <50 <50 <50 <0.1 NA 9-Mar-06 1200 <50 <50 <50 4 86 14-Jun-06 1100 <50 <50 <50 5.2 116 20-Jul-06 1120 <50 <50 <50 4.3 123 8-Nov-06 1050 1.6 2.6 <1 4.6 134 28-Feb-07 1200 1.3 <1 <1 4 133 27-Jun-07 1800 2.3 15-Aug-07 1100 1.9 <1 <1 4.1 129 10-0ct-07 1100 1.9 <1 <1 4 132 26-Mar-08 1800 2.9 <1 <1 2.2 131 25-Jun-08 1000 1 <1 <1 2.81 128 10-Sep-08 3600 8.6 <1 <1 36.2 113 15-0ct-08 4200 12 <1 <1 47.8 124 4-Mar-09 1100 1.2 <1 <1 3.2 127 24-Jun-09 990 1.2 · <1 <1 2.4 132 15-Sep-09 6600 15 <1 <1 0.1 43 14-Dec-09 4700 16 <1 <1 26.7 124 17-Feb-10 940 1.3 <1 <1 2 144 9-Jun-10 1800 4.2 <1 <1 4.4 132 16-Aug-10 2000 4.9 <1 <1 5.9 142 3400 17 17 7-Jun-ll 4000 8.3 ND ND 12 148 17-Aug-ll 970 2.1 ND ND 3 148 5-Dec-ll 2200 5.4 ND ND 5 148 23-Jan-12 650 1.5 ND ND 0.6 138 6-Jun-12 460 1.1 ND ND 2.4 149 5-Sep-12 950 3.5 ND ND 2.5 149 f~rIJ~' , ~~"'~'Di'y.lell ':,~ 10 ' ,rome e* :'l ',~~~, ,1i.g ''fetrac< ( 7'1) bloride ~~ ,.Aii ' :1 (mgfil~, '.~ .I'i!l}... ~ ~ ."" I 'ill' i" ' '(U,2f.1~,. ~, l~" ~; ug ,:~"(~~fI)': itJ III .':L.'" 3': "",", Jit'-, 25-May-05 39000 NA NA NA 10.1 NA 31-Aug-05 3800 <10 <10 <10 2.9 NA I-Dec-05 19000 <250 <250 <250 1.8 NA 9-Mar-06 9200 <500 <500 <500 3.8 120 14-Jun-06 61000 <500 <500 <500 9.4 235 20-Jul-06 ' 5300 <1000 <1000 <1000 2.9 134 8-Nov-06 11000 7.1 1.9 2.2 3.5 124 28-Feb-07 4400 3.1 <1 1.1 4.2 124 27-Jun-07 1800 2.2 <1 <1 2.3 112 15-Aug-07 5200 3.5 <1 1.8 2.1 117 10-0ct-07 9000 6.8 <1 1.9 5.6 170 26-Mar-08 13000 9 <1 1.5 0.9 132 25-Jun-08 30000 13 <1 1.2 7.96 191 10-Sep-08 21000 15 <1 3.7 4.44 156 15-0ct-08 NA NA NA NA 5.51 166 4-Mar-09 8200 5.7 <1 5.2 5.1 164 24-Jun-09 6800 4.9 <2 4.2 2.9 164 15-Sep-09 13000 8.4 <2 4.4 3.3 153 14-Dec-09 15000 14 <1 3 5.3 187 17-Feb-l0 3500 2.7 <1 3.2 2 179 14-Jun-l0 18000 11 <1 3.7 5.6 200 16-Aug-l0 15000 12 <1 2.2 5.3 196 11-0ct-l0 24000 20 <1 5.5 4.6 203 23-Feb-ll 31000 27 ND 19 4.4 220 I-Jun-ll 8100 10 ND 2.1 4.8 177 17-Aug-ll 6800 7.3 ND 3.1 6.5 207 16-Nov-ll 7900 7.2 ND 2.5 4.2 186 23-Jan-12 11000 10 ND 1.3 7.9 207 6-Jun-12 36000 33 ND ND 11 262 4-Sep-12 13000 26 ND ND 10.8 289 <1 <1 <1 <1 <0.1 46 <1 <1 <1 <1 <0.1 43 26-Mar-08 <1 <1 <1 <1 <0.1 41 25-Jun-08 <1 <1 <1 <1 <0.05 41 10-Sep-08 <1 <1 <1 <1 <0.05 35 15-0ct-08 <2 <2 <2 <2 <0.05 51 4-Mar-09 <1 <1 <1 <1 <0.1 41 24-Jun-09 <1 <1 <1 <1 <0.1 43 15-Sep-09 <1 <1 <1 <1 <0.1 43 16-Dec-09 <1 <1 <1 <1 <0.1 37 24-Feb-l0 <1 <1 <1 <1 <0.1 45 8-Jun-l0 <1 <1 <1 <1 <0.1 40 10-Aug-l0 <1 <1 <1 <1 <0.1 40 5-0ct-l0 <1 <1 <1 <1 <0.1 34 16-Feb-ll ND ND ND ND ND 44 25-May-ll ND ND ND ND ND 44 16-Aug-ll ND ND ND ND ND 41 15-Nav-ll ND ND ND ND ND 43 17-Jan-12 ND ND ND ND ND 40 31-May-12 ND ND ND ND ND 44 29-Aug-12 ND ND ND ND ND 46 TabL Chloroform Concentration Trend Graphs o """"" o o o N o o o (ug/L) VJ o o o J:::o,. o o o 0'1 o o o m o o o Sep-99 l » ••• Dec-99 Mar-OO Jun-OO Sep-OO Dec-OO Mar-01 Jun-01 Sep-01 Dec-01 Mar-02 Jun-02 Sep-02 Dec-02 Mar-03 Jun-03 ~;j~l!t I · 7 Dec-04 Mar-05 Jun-05 Sep-05 Dec-05 Mar-06 Jun-06 Sep-06 Dec-06 Mar-O? Jun-O? Sep-O? Dec-O? Mar-08 Jun-08 Sep-08 Dec-08 Mar-09 Jun-09 Sep-09 Dec-09 Mar-10 Jun-10 Sep-10 Dec-10 Mar-11 Jun-11 Sep-11 Dec-11 Mar-12 Jun-12 --...J o o o ~ ____ '~I __ ~~~~ ______ L-____ ~ ____ ~ ______ ~ ____ ~ s:: ~ I () :::J'" o a cr ., 3 ~ c CD CJ) rn CI) ::::s C'CS > E ~ ~ 0 ~ .2 .c 0 T"" I oq- 3: I- ~----~------~------r-----~------~------~----~v~-~aa-Lc 60-lnr-9 90-PO-O~ vo-uer-v~ 1-----1-----1----+-----+----+----+---+ 86-lnr-vc o o o I'- o o o CO o o o LO o o o 'o;;t o o o ('I') o o o N o o o o TW4-2 Chloroform Values 7000 ~--------------------------------------------------------------------------------~ 6000 I • 5000 I 1\, .... '. I " A 4000 I \;, , ,~ It.. • ......--~ I , ~ 'A' '\ •. ~ • ...J < -C) :::s -3000 I 2000 1 I I \ I Data point represented corresponds to laboratory results. The value is 1000 I I likely underestimated due to 0 ex> T""" 0> 0 ....!.. I L.. :J a. -, « I ~ I N 0> laboratory error not considering the dilution factor of 10. ~ CD 0 0 I I C 1:5 ro 0 -, I I ~ 0 0> 0 I "3 -, I CD N ~ T""" T""" I I L.. () a. (]) <} 0 I I'-N tn CI) ::::s C'CS > E ~ .e 0 0 ~ .2 .c 0 M I oq- I 3: ~ U> Cl) :::l co > E ... ~ 0 ... ..2 ..c: 0 -.::t I ~ I- r------r----,-----,---~--__r_--_r__--..,.__--r__-___._ £; ~ -on\;f-v ~ o ~-I\ON-S ~ 60-l nr-9 SO-qa.::J-ll 90-PO-O~ 90-Aell'J-Sl vo-uer-v~ lo-das-~ ~1--t---+--k_J ~O-Jd\;f-6 ~ 66-::>aO-9 t-----t---t----t----t---t-----t---t----i---+ S6-l nr-vl o o L{) ~ o o o ~ o o L{) ('I) o o o ('I) o o L{) N (1/6n) o o o N o o L{) o o o o o L{) o 1 tn Q) :J ns > E ... ~ 0 ... .2 .t: 0 LO I ~ 3: t- ~----~------~----~------~------~-----r----~v~-oaa-LG 60-lnr-9 90-PO-O~ vo-uer-V~ I-----+----+-----+----i-----+----I-------I-B6-lnr-vG o LO ('t) o o ('t) o LO N o o N o LO (1/6n) o o o LO o tn CJ) :::s cu > E ... ~ 0 ... .2 .c 0 CD I ~ 3: .- ,-----..,----...,------r-------,.----,-----,-£ ~/v~/SO l~HOlvO 60/90lLO SOlllllO 9010 ~/O ~ 90/Sll90 vOlv~/~O lOHO/60 ~0/6 ~/vO 66/901l~ !-----i------+----t-----t-----+----..........r-S61vllLO o o N o o o o o ex:> o o CD o o ""'" o o N o U) CI) ::::s ns > E ... ~ 0 ... .2 .c 0 '" I ~ ~ I- ~------~--------~--------r-------~--------~------~v~-~aa-LG o o o CD o o o L(') o o o ~ o o o ('f) o o o N o o o o 60-lnr-9 90-PO-O~ vo-uer-v~ ~ tn Cl) ~ co > E ... ~ 0 ... £ .c 0 co I "II:t 3: I- .-----r----r----r------'-',------,----,---..,.---__ r----r----r V ~ -:>eo-Ll 60-lnr-9 90-PO-O~ vo-uer-v~ I----+---;---+----t----;---i---+---;---+----+ B6-lnr-vl o o L{) o L{) ~ o o ~ o L{) ('t) o o ('t) o L{) N o o N o L{) o o o L{) o ~ tn (J) ~ ns > E ... ~ o ... .2 s::. (J en I ~ ,...----r-------r------,-----,-----,-----,--------r V ~-::>ea-L2 60-lnr-9 vo-uer-v~ t------I-----+-----+---.......,..---......j-----i-----+ 86-lnr-vl o CO o L() (1/6n) o ('t) o N o o tn Cl) :::l CO > E ... ~ 0 ... .2 .t: 0 0 "'(- I ~ 3: I- ,...-----,----....,.-----r-------,-----,----....,..----r £ ~ -6n'v'-v~ o o "'" o o N o o o o o CO o o CO o o "'" o o N o O~-AON-B~ 60-l nr-9 BO-qa.:l-GG 90-PO-O~ 90-Aell\l-BG vo-uer-v~ Go-das-~ rn Cl) :1 co > E ... J2 0 ... .2 .c 0 ~ ~ I ~ ~ ~ a a a I"'-- a a a (0 a a a L() a a a ~ a a a ('I') a a a N a a a a o ~-J\ON 8 ~ 80-qe.::J II 90-PO-~ 90-AeV\l 8l vo-uer-~ lo-des ~ a a a T""" I ~ o ~ 0'1 (ug/L) 6 0, N o 19-Apr-01 -t-I------+--------+------+--------I 1-Sep-02 14-Jan-04 28-May-05 10-0ct-06 22-Feb-08 6-Jul-09 18-Nov-10 1-Apr-12 14-Aug-13 -L-_____ .....l.-______ ---!. ______ ..I-_____ ..... -f ~ I ~ I\) 0 ::r 0" .., 0 0' .., 3 < S» C CD fA Sep-02 Dec-02 Mar-03 Jun-03 Sep-03 Dec-03 Mar-04 Jun-04 Sep-04 Dec-04 Mar-05 Jun-05 Sep-05 Dec-05 Mar-06 Jun-06 Sep-06 Dec-06 Mar-07 Jun-07 Sep-07 Dec-07 Mar-08 Jun-08 Sep-08 Dec-08 Mar-09 Jun-09 Sep-09 Dec-09 Mar-10 Jun-10 Sep-10 Dec-10 Mar-11 Jun-11 Sep-11 Dec-11 Mar-12 Jun-12 o ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ H ~ ~ ~ ~ ~ H ~ " ~ " ~ " ~ " " " ~ ~ " H ~ " ~ " ~ H 9 9 N 9 w o ~ (ug/L) o 0'1 () :::J'" 0 ..., 0 0' ..., 3 :::J'" Q) en :::J 0 r"+' c-eo eo :::J a. eo r"+' eo (') r"+' eo a. :::J -I ~ ~ I .....li.. W o m o -....,J 9 co 9 CD -I ~ I ....lo W o :::r 0" (3 0' -a 3 < S» C (I) en ~~ ~. ~~ ~. ~. ~ ~ I ~ ~~ $ O~-AON-S~ r-~ c ~ .-~ "'C Q) ~ ~ +-' U ~ Q) +-' Q) ~ "'C ~ 60-lnr-9 C Q) H Q) .c +-' ~ 0 ~ C ~ Ul CO ~ ..c SO-qa.:l-ZZ E s..... ~ ~ ~ 0 ~ s..... 0 ~ -..c 0 ~ 90-PO-O~ 90-ABV\I-S( o o o o o (1/6n) U> CI) :::l cu > E ... ~ 0 ... .2 J: 0 CD N I ~ :E ...-----...,..---~----_,_---,___--___r"---__r_---.....__ £ ~ -6n'v'-v ~ o ~-J\oN-S~ 60-lnr-9 SO-qe.:l-ll 90-PO-O~ 90-AeV\l-Sl !-----+-----+-----+-----+-----I-----I------+ vo-uer-V~ o o LO ('I') o o o ('I') o o LO N o o o N o o LO o o o o o LO o o ~ o o N o o (ug/L) w o o .J:::o. o o (]I o o 0> o o 19-Apr-01 +I----+-------!------+-----+-----+------I 1-Sep-02 14-Jan-04 28-May-05 1 O-Oct-06 -I ~ I 22-Feb-08 -I l.. II 6-Jul-09 18-Nov-10 1-Apr-12 14-Aug-13 -.J -t :e ~ I ~ en 0 :::r 0 ~ 0 0' ~ 3 < S» c (1) til tn Q) :::l CO > E ... ~ 0 ... .2 .c 0 N M I 3: :E .------r----,----,----r----,----,...-------,-----r-----r £ ~ -on'v'-v ~ l ~ -Jd'v'-~ ~ ~ ~ ~ ~ ~ ~ ~ O~-AoN-8~ ~ ~ ~ ~ ~ ~ ~~ 60-lnr-9 ~ n 0 ~~ 80-qe.:l-ll 0 0 0 0 ~~ 90-PO-O~ a 0 ~~ ~~ ~~ SO-Aell\l-8l 0 0 ~~ ~~ 0 vo-uer-v~ 0 ~~ ~~ ~~ lo-des-~ \----I----/-----+----+---+---+----I----+---_+_ ~O-Jd'v'-6 ~ co o co o N o o tn Cl) ::l co > E .... ~ 0 .... ..2 J: 0 co ~ I 'III:t ~ ~ ,...-----,..---,.-----,..---,.-----,..---,..-----,----,.-----,..---y-£ ~ -6n'v'-v ~ 60-lnr-g 80-qa.::J-ll 9O-PO-O~ SO-ABV\I-8l VO-UBr-v~ lo-das-~ 1----+---+----+---+---I---+---!---+---+---4-~O-Jd'v'-6 ~ o o L() o L() ~ o o ~ o L() ('t') o o ('t') o L() N o o N o L() ~ o o o L() o r----....,...-----,.----r------r----"r----...,.-----r--------, £ ~-6n'V-v~ o ~-J\oN-S ~ tn 60-lnr-9 CI) ::::s co > E ... ~ 0 ... .2 .£:: so-qa.::J-C;C; 0 en 't"'" I ~ 3: I- 90-PO-O~ 90-AeV\l-SC; vo-uer-v~ 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 co t-eo LO -.::t ('I') N (1/6n) r------r---_r__---~--_r_---_r__---~--_r £ ~-6n'V-v~ O~-AON-9~ tn 60-lnr-9 Cl) ::::s ca > E ... ~ 0 ... .2 90-qa=l-ll .c 0 0 N I ~ 3: I- 90-PO-O~ 90-AeV\l-9l vo-uer-v~ 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 r--(0 LO ...:t ('t') C\I -r- (1/6n) fA CI) ~ CU > E ~ ~ 0 ~ .2 .c U ~ N I ~ 3: I- ,.------,----r-----,----r----,----r-----r---..,...-----r---..,-£ ~ -6n'v'-v ~ o o LO o LO ~ o o ~ o LO ('t) o o ('t) o LO N o o N o LO o o o LO o o ~-J\oN-B~ 60-lnr-9 BO-qa=f-ll 90-PO-O~ 90-AeV\l-Bl en Q) ::::J cu > E ... ~ 0 ... .2 ..c 0 N N I ~ := I- O~-J\ON-B ~ 60-lnr-g BO-qa.:l-ll 90-PO-O~ 90-AeV\l-Bl I-----..J----....J.-...----+------I-----+----~---_+ vo-uer-v~ o o o I'- o o o <.0 o o o IJ') o o o -.::t o o o ('I) o o o N o o o o o o o Jun-07 Sep-07 Dec-07 Mar-08 Jun-08 Sep-08 Dec-08 Mar-09 Jun-09 Sep-09 Dec-09 Mar-10 Jun-10 Sep-10 Dec-10 Mar-11 Jun-11 Sep-11 Dec-11 Mar-12 ~ (ug/L) o o () :::J'" 0 ...., 0 0' ...., 3 :::J'" Q) en :::J 0 ,..-+. e- CD CD :::J a. CD ,..-+. CD (') ,..-+. CD a. :::J --I ~ I i') W ~ I I\) W o ::T 0" "'" o 0' "'" 3 < Q) c CD tA ....------.-----...,.--------r-------.------,-------,..---------,... E"[-8nv-p"[ O"[-J\ON-8"[ 60-l nr-9 80-qa:/-u: '-___ ....L--___ --'-___ ---I ___ ._--.l. ____ .l....-___ ...L..-. ___ .--l.. 90-PO-O"[ o m IJ') N o N IJ') .-i o .-i IJ') o o o o o o o o Jun-07 0 0 Sep-07 0 Dec-07 Mar-08 ~~ Jun-08 0 Sep-08 0 0 Dec-08 Mar-09 ~~ Jun-09 0 Sep-09 0 Dec-09 0 0 Mar-10 Jun-10 0 0 Sep-10 0 Dec-10 0 Mar-11 0 Jun-11 ~~ Sep-11 ~~ Dec-11 0 Mar-12 0 Jun-12 Sep-12 ~~ (ug/L) (") ::::r 0 .., 0 0' .., 3 ::::r Q) CJ) :::J 0 r-+ e-CD CD :::J a. CD r-+ CD (") r-+ CD a. _. :::J --i ~ ~ I I'V 01 --- ~ I I'\) en o :::T 0" ... o 0' ... 3 < S» C (1) tn 0 N ~ T Jun-l0 Jul-l0 Aug-l0 Sep-l0 Oct-l0 Nov-l0 Dec-l0 Jan-ll Feb-ll Mar-ll Apr-ll May-ll Jun-ll Jul-ll Aug-ll Sep-ll Oct-ll Nov-ll Dec-ll Jan-12 Feb-12 Mar-12 Apr-12 May-12 Jun-12 Jul-12 Aug-12 Sep-12 (ug/I) 0'\ 00 ...... o ...... N ...... ~ ..... :E ~ I N 0\ n :::r 0" ~ o 0' ~ 3 < D) C tD U) ll-qa::l '-~ ll-uer (1/8n) TabM CSV Transmittal Letter Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Lundberg, Kathy Weinel Monday, November 26,20129:31 AM 'rlundberg @ utah.gov' Dean Henderson; 'Phillip Goble'; Harold Roberts; David Frydenlund; Jaime Massey; David Turk; Jo Ann Tischler Transmittal of CSV Files White Mesa Mill 2012 03 Chloroform Monitoring C12081321.csv; C12090222.csv; C12090481.csv Attached to this e-mail is an electronic copy of laboratory results for chloroform monitoring conducted at the White Mesa Mill during the third quarter of 2012, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel 1