DAQ-2024-004265

1

DAQC-028-24
Site ID 10346 (B4)

MEMORANDUM

TO: STACK TEST FILE – KENNECOTT UTAH COPPER – Smelter

THROUGH: Harold Burge, Major Source Compliance Section Manager

FROM: Paul Morris, Environmental Scientist

DATE: January 9, 2024

SUBJECT: Source: FSF Dry Feed Bin Baghouse - SME005
Contact: Sean Daly: 801-204-2563
Location: Kennecott Smelter Facility, Magna, Salt Lake County, UT
Test Contractor: Alliance Technical Group.
FRS ID #: UT0000004903500030
Permit/AO#: Title V Operating Permit 3500030004, dated September 18,
2020, and DAQE-AN103460061-22, dated June 23, 2022
Action Code: 3A
Subject: Review of Stack Test Report dated December 19, 2023

On December 20, 2023, Utah Division of Air Quality (DAQ) received a test report for the Kennecott Utah
Copper FSF Dry Feed Bin Baghouse Stack. Testing was performed on October 25, 2023, to demonstrate
compliance with the emission limits found in AO Condition II.B.1.a and Permit Condition II.B.6.a. The
DAQ-calculated test results are:

Source Test Date Test Method Pollutant Result Limit

SME005 10/25/2023 5/202 PM10 0.003 grain/dscf 0.016 grain/dscf
0.04 lb/hr 1.2 lb/hr

DEVIATIONS: Method 5 was conducted in lieu of Method 201A. Method 201A requires
a minimum stack diameter to meet blockage requirements. UDAQ has
approved this approach in the past.

CONCLUSION: Kennecott Utah Copper appears to be in compliance with the applicable
conditions of the Title V operating permit at the time of this test.

RECOMMENDATION: Kennecott Utah Copper should be considered in compliance with the
emission limits listed.

HPV: No violations occurred.

ATTACHMENT: Stack test report dated December 19, 2023, DAQ spreadsheets

6 , 3
Mr. Bryce Bird - Director
Department of Environmental Quality
Division of Air Quality
P.O. Box 144820
Salt Lake City, Utah 84114-4820
December 19,2023
Attn: Joe Randolph
Rio Tinto Kennecott Utah Copper, LLC
4700 Daybreak Parkway
South Jordan, Utah 84009
TITAH DEPAHTMENT OF
ENVIRONMENTAL OUAIJTV
lrl- I it ll 'ri"j3
ilor/ 'l)r-ti'teftcl
DIVISION OF AIR QUALITY
Subject: Stack Test Report - Kennecott Utah Copper Smelter
Flash Smeltino Furnace Drv Feed Bin Baohouse SME005
Title V Operating Permit No. 3500030004
Dear Mr. Bird,
As required by Title V operating permit 3500030004 and Approval Order DAQE-
AN103460060-21 , Kennecott Utah Copper performed a particulate performance stack test of
the Flash Smelting Furnace Dry Feed Bin Baghouse (SME005) on October 25,2023. The
testing was conducted following procedures outlined in 40 CFR 60, Appendix A. The
summary report with test results is attached for submittal within 60 days of completion of the
testing. Results of the testing demonstrate that the unit is in compliance with the permit
emission limits.
Based on information and belief formed after reasonable inquiry, the statements and information
in this document are true, accurate, and complete (R307-415-5d).
lf you have any questions regarding this report, please contact me or Sean Daly at 801-569-6331.
Yours sincerely,
o.ru
Jerome Dozol
General Manager - Metals
Rio Tinto Kennecott Utah Copper, LLC. 4700 Daybreak Parkway, South Jordan, Utah 84009.
*l
r#9T.""-',ffi
'f1P****"
tru
i\l : I , i*1
UTAH DEPAHTI,IINT OF
ENVIRONME,NTAL OUAUTY
Source Test Report
Rio Tinto Kennecott DIVISION OF AIR QUALITY
4700 Daybreak Parkway
South Jordan, UT 84095
Source Tested: Flash Smelting Furnace Dry Feed Bin
Baghouse SME005
Test Date: October 25,2023
Project No. AST-2023-3 17 9 -002
Prepared By
Alliance Technical Group, LLC
3683 W 2270 S, Suite E
West Valley City, UT 84120
piltffirpe
TECI-i NICAL GROUP Source Test Report
Test Prosram Summan)
Regulatory Information
Permit Nos.
Source Information
DAQE-AN1034600s6-20
Title V Operating Permit 3500030004
Source Name
Flash Smelting Furnace Dry Feed
Bin Baghouse
Contact Information
Source ID
SMEOO5
Target Parameters
PMlO, CPM
Test Location Test Company Analytical Laboratories
Kennecott Utah Copper, LLC Alliance Technical Group, LLC Alliance Technical Group, LLC
4700 Daybreak Parkway 3683 w 2270 s, Suite E 5530 Marshall street
South Jordan, UT 84009 West Valley City, UT 84120 Arvad4 CO 80002
Eric Grosjean
Jenny Esker Project Manager [e-mail]@riotinto.com Charles Horton (303) 420-5g4g
[phone] [e-mail]
Sean Daly Q52) 663-7568 Particle Technologv Labs
555 Rogers [e-mail] Field Team Leader Downers Grove, IL 60515
[phone] lobias Hubbard Oliver Urbanek
[e-mail] [e-mail]
(605) 64s-8s62 [phone]
QA/QC Manager
Kathleen Shonk
katie.shonk@,alliancetg.com
(812) 4s2-478s
Report Coordinator
Delaine Spangler
[e-mail]
RTK - Magna, UT
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AST-2023-3179-002 Page i
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TEC}-JNICAL GROUP Source Test Report
C e rt i fi c ati on Sta te me nt
Alliance Technical Group, LLC (Alliance) has completed the source testing as described in this report. Results
apply only to the source(s) tested and operating condition(s) for the specific test date(s) and time(s) identified within
this report. All results are intended to be considered in their entirety, and Alliance is not responsible for use ofless
than the complete test report without written consent. This report shall not be reproduced in full or in part without
written approval from the customer.
To the best of my knowledge and abilities, all information, facts and test data are correct. Data presented in this
report has been checked for completeness and is accurate, error-free and legible. Onsite testing was conducted in
accordance with approved internal Standard Operating Procedures. Any deviations or problems are detailed in the
relevant sections in the test report.
This report is only considered valid once an authorized representative ofAlliance has signed in the space provided
below; any other version is considered draft. This document was prepared in portable document format (.pdf) and
contains pages as identified in the bottom footer of this document.
-/ J.t
,/irj
/"-n"/"
i$1,,
12n9t2023
Charles Horton, QSTI
Alliance Technical Group, LLC
Date
AST-2023-3 I 79-002 Page iiRTK- Magra, UT
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piltfrnoe
TECI.lNICAL GROUP Source Test Report
Table ofContents
TABLE OF CONTENTS
1.1 Process/Control System Descriptions. ................. 1-1
1.3 Site-Specific Test Plan & Notification................... ................... l-1
3.1 U.S. EPA Reference Test Methods I and2- Sampling/Traverse Points and Volumetric Flow Rate........3-l
3.2 U.S. EPA Reference Test Method 4 - Moisture Content......... ....................... 3-l
3.3 U.S. EPA Reference Test Methods 5 and202 - Total Particulate Matter........... ..................3-l
LIST OF TABLES
APPENDICES
Appendix A Sample Calculations
Appendix B Field Data
Appendix C Laboratory Data
Appendix D Quality Assurance/Quality Control Data
Appendix E Process Operating/Control System Data
AST-2023-3l't9-002 Page iiiRTK - Magna, UT
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l-:c Source Test Report
Introduction
1.0 Introduction
Alliance Technical Group, LLC (Alliance) was retained by Rio Tinto Kennecott (RTK) to conduct compliance
testing at the Smelter facility in Magna, Utah. Portions of the facility are subject to provisions of the Utah
Department of Environmental Quality, Division of Air Quality (UDAQ) Approval Order (AO) DAQE-
AN103460056-20 and the Title V Operating Permit No. 3500030004. Testing was conducted to determine the
emission rates of filterable particulate matter less than l0 microns (PMIO) and condensable particulate matter
(CPM) from the exhaust of the Flash Smelting Furnace (FSF) Dry Feed Bin Baghouse designated as SME005. Due
to the 17.5inch stack diameter, Method 5 was conducted in lieu of method 2014. Method 20lA required a
minimum stack diameter of 17.6 inches to meet blockage requirements per the EPA FAQ on Method 201A. Particle
sizing was conducted using scanning electron microscopy (SEM) to determine PMIO. CPM emissions were
collected for inventory purposes only and shall not be used for compliance demonstration.
Flow fluctuations observed at the stack make isokinetic flow sampling impossible as outlined in EPA Methods 5 and
202; therefore, a deviation from the test methodology is required. Prior to testing, flow measurements will be
collected over a one-hour period and used as the flow rate during the compliance testing program. UDAQ has
approved this approach in the past.
1.1 Process/ControlSystemDescriptions
Product leaving the concentrate rotary dryer is delivered in an enclosed pneumatic transfer to the FSF feed bin. Dry
feed bin loading, bin discharge points, and chain conveyors are vented to a baghouse (SME005).
1.2 Project Team
Personnel involved in this project are identified in the following table.
Table 1-1: Project Team
1.3 Site-Specific Test Plan & Notification
Testing was conducted in accordance with the Site-Specific Test Plan (SSTP) submitted to UDAQ by RTK.
RTK Personnel Sean Daly
Alliance Personnel
Tobias Hubbard
Taylor Gentry
Travis Hebert
AST-2023-3 l 79-002 Page l-1RTK - Magna, UT
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TECI"-lNICAL GNOt]P Source Test Report
Summary of Results
2.0 Summary of Results
Alliance conducted compliance testing at the RTK Smelter facility in Magna, Utah on October 25, 2023 . Testing
consisted of determining the emission rates of filterable PMl0 and CPM from the exhaust of the FSF Dry Feed Bin
Baghouse designated as SME005. Due to the 17.5inch stack diameter, Method 5 was conducted in lieu of method
201A. Method 20lA required a minimum stack diameter of 17.6 inches to meet blockage requirements per the EPA
FAQ on Method 201A. Particle sizing was conducted using scanning electron microscopy (SEM) to determine
PM10. CPM emissions were collected for inventory purposes only and shall not be used for compliance
demonstration.
Flow fluctuations observed at the stack make isokinetic flow sampling impossible as outlined in EPA Methods 5 and
2021' therefore, a deviation from the test methodology is required. Prior to testing, flow measurements were
collected over a one-hour period and used as the flow rate during the compliance testing program. UDAQ has
approved this approach in the past.
Table 2-1 provides a summary of the emission testing results with comparisons to the applicable UDAQ permit
limits. Any difference between the summary results listed in the following table and the detailed results contained in
appendices is due to rounding for presentation.
Table 2-1: Summary of Results
terable Particulate Matter Data
Concentration, grain/dscf
Emission Rate, lb/hr
rable Particulate Matter less than 10 Microns Da
Concentration, grain/dscf
Emission Limit, grain/dscf
Percent of Limit, 7o
Emission Rate, lb/hr
Emission Limit, lb/hr
Percent of Limit, 7o
0.00032
0.0049
0.00053
0.0088
0.00023
0.0041
0.00036
0.016
2
0.0059
1.25
<1
densable Particulate Matter Data
Concentration, grain/dscf
Emission Rate, lb/hr
AST-2023-3 I 79-002 Page 2-lRTK-Mapa, UT
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Source Tesl Report
Testing Methodoloxy^
3.0 Testing Methodology
The emission testing program was conducted in accordance with the test methods listed in Table 3-1. Method
descriptions are provided below while quality assurance/quality control data is provided in Appendix D.
Table 3-l: Source Testing Methodology
3.I U.S. EPA Reference Test Methods 1 and 2 - Sampling/Traverse Points and Volumetric Flow Rate
The sampling location and number of traverse (sampling) points were selected in accordance with U.S. EPA
Reference Test Method l. To determine the minimum number of traverse points, the upstream and downstream
distances were equated into equivalent diameters and compared to Figure l-1 in U.S. EPA Reference Test Method 1.
Full velocity traverses were conducted in accordance with U.S. EPA Reference Test Method 2 to determine the
average stack gas velocity pressure, static pressure and temperature. The velocity and static pressure measurement
system consisted of a pitot tube and inclined manometer. The stack gas temperature was measured with a K-type
thermocouple and pyrometer.
The O: and COz concentration were assumed to be ambient for molecular weight and volumetric flow rate
calculations.
Stack gas velocity pressure and temperature readings were recorded during each test run. The data collected was
utilized to calculate the volumetric flow rate in accordance with U.S. EPA Reference Test Method 2.
3.2 U.S. EPA Reference Test Method 4 - Moisture Content
The stack gas moisture content (BWS) was determined in accordance with U.S. EPA Reference Test Method 4. The
gas conditioning train consisted of a series of chilled impingers. Prior to testing, each impinger was filled with a
known quantity of water or silica gel. Each impinger was analyzed gravimetrically before and after each test run on
the same balance to determine the amount of moisture condensed.
3.3 U.S. EPA Reference Test Methods 5 and 202 -Total Particulate Matter
The total particulate matter (filterable and condensable PM) testing was conducted in accordance with U.S. EPA
Reference Test Methods 5 and 202. The complete sampling system consisted of a glass nozzle, glass-lined probe,
pre-weighed quartz filter, coil condenser, un-weighed Teflon filter, gas conditioning train, pump and calibrated dry
gasmeter. Thegasconditioningtrainconsistedofacoiledcondenserandfour(4)chilledimpingers. Thefirst,and
second impingers were initially empty, the third contained 100 mL of de-ionized water and the last impinger
contained 200-300 grams of silica gel. The un-weighed 90 mm Teflon filter was placed between the second and
third impingers. The probe liner heating system was maintained at a temperature of 248 +25'F, and the impinger
temperature was maintained at 68oF or less throughout testing. The temperature of the Teflon filter was maintained
greater than 65oF but less than or equal to 85'F.
RTK - Magna. UT
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Parameter tl;S, EP! Refeience
Test Methods Notes/Remarks
Volumetric Flow Rate 1&2 Full Velocity Traverses
Moisture Content 4 Gravimetric Analvsis
Total Particulate Matter 51202 Constant Rate Sampling
AST-2021-r179-002 Page 3-1
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TECI-I NICAL GROUP Source Test Report
Testing Methodology
Following the completion of each test run, the sampling train was leak checked at a vacuum pressure greater than or
equal to the highest vacuum pressure observed during the run. The nitrogen purge was omitted due to minimal
condensate collected in the dry impingers. After the leak check the impinger contents were measured for moisture
gain.
The pre-weighed quartz filter was carefully removed and placed in container 1. The probe, nozzle and front half of
the filter holder were rinsed three (3) times with acetone to remove any adhering particulate matter and these rinses
were recovered in container 2. All containers were sealed, labeled and liquid levels marked for transport to the
identified laboratory for filterable particulate matter analysis.
The contents of impingers I and2 were recovered in container CPM Cont. #1. The back half of the filterable PM
filter holder, the coil condenser, impingers I and 2 and all connecting glassware were rinsed with DruF water and
then rinsed with acetone, followed by hexane. The water rinses were added to container CPM Cont. #l while the
solvent rinses were recovered in container CPM Cont. #2. T\e Teflon filter was removed from the filter holder and
placed in container CPM Cont. #3. The front half of the condensable PM filter holder was rinsed with DIUF water
and then with acetone, followed by hexane. The water rinse was added to container CPM Cont. #1 while the solvent
rinses were added to container CPM Cont. #2. All containers were sealed, labeled and liquid levels marked for
transport to the identified laboratory for condensable particulate matter analysis.
RTK- Magna, UT
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AST-2023-3 1 79-002 Page 3-2
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TTCHNICAL *NOLJP
Location: Rio Tinto Kennecott - Magna, UT
Appendix A
Example Calculations
Source: Flash Smeltins Furnace Dry Feed Bin Bashouse SME005
Project No.: AST-2023-3179
Run No.: I
Parameter: PM
Meter Pressure (Pm), in. Hg
AHPm = Pb+'
13.6
where,
Pb@= barometric pressure, in. Hg
AH 1.133 = pressure differential oforifice, in H2O
Pm 26.96 = in. Hs
Absolute Stack Gas Pressure (Ps), in. Hg
Po
Ps = Pb + '"
where, 1? 6
Pb 26.88 = barometric pressure, in. Hg
Pg 0.46 = static pressure, in. H2O
Ps 26.91 = in. HB
Standard Meter Volume (Vmstd), dscf
77.636xYxVmxPm
Vmstd =where,Tm
Y 1.05 = meter correction factor
Vr-]!Q[= meter volume, cf
P^ @= absolute meter pressure, in. Hg
Tm 567.1 = absolute meter temperature, oR
Ym516-Jlll[f =65s1
Standard Wet Volume (Vwstd), scf
Vwstd = 0.04716 x Vlc
where ,
Vlc 16.2 = weight of H2O collected, g
v*rtd ---674-= r"f
Moisture Fraction (BWSsat), dimensionless (theoretical at saturated conditions)
Ts 164.1 : stack temperature, oF
Pr@= absolute stack gas pressure, in. Hg
BWSsat 0.390 : dimensionless
Moisture Fraction (BWS), dimensionless (measured)
Vwstdnttra
*n.".f ' (Vwstd * Vmstd)
Vwstd ...;[fu = standard wet volume, scf
Vmstd
-!!![=
standard meter volume, dscf
Bws '.4= dimensionless
Moisture Fraction (BWS), dimensionless
BWS = BWSmsd unless BWSsat < BWSmsd
where,BWSsat..;fu= moisture fraction (theoretical at saturated conditions)
BWSmsd ..1!Q[ = moisture fraction (measured)
BWS 0.022
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,ousz_(1!ffi)
BWSsat =
-where, P'
pllrffiirce
TECHNlCAL CNOUi]
Appendix A
Example Calculations
Location:
Source:
Project No.:
Run No.:
Parameter:
Rio Tinto Kennecott - Magna, UT
Flash Smeltins Furnace Dry Feed Bin Bashouse SME005
AST-2023-3179
PM
Molecular Weight (DRY) (Md), lbflb-mole
Md =(0.44x0/oco2)
where,
0l
+ (0.32 x 0/oOZ) + (0.28 (100 - o/oCO2 - o/oO2))
= carbon dioxide concentration,Yo
20.9 = oxygen concentration, o/o
Md 28.85 = lb/lb mol
Molecular Weight (WET) (Ms), lbflb-mole
Coz
o2
Ms=
where,
Vs=
where,
Md (1 - BWS) + 18.01s (BWS)
Md@= molecularweight (DRY), lb/lb mol
BWS ..;!Q[: moisture fiaction, dimensionless
Ms 28.62 = lb/lb mol
Average Velocity (Vs), ftlsec
85.49 x Cp x (LYttzlavg x
Cp 0.840 = pitot tube coefficient^
A P"'.A=vetocityhead of stack gas' (in H2o)t/2
T...1@$-= absolute stack temperature, oR
Ps-zqL= absolute stack gas pressure, in. Hg
Mt &= molecular weight of stack gas, lb/lb mol
Vs 24J = n7r..
Average Strck Grs FIow at Stack Conditions (Qa), acfm
Qa=60xVsxAs
where,Vs 24.1 : stack gas velocity, ff/sec
As 1 .67 = cross-sectional area of stack, ft2QuE=u.r,
Average Stack Gas Flow at Standrrd Conditions (Qs), dscfm
Ps
Qs = 17.636 x Qa x (1 - BWS) * *where,
Qa_W_= average stack gas flow at stack conditions, acfm
BWS ..;!Q[= moisture fraction, dimensionless
Pr_@= absolute stack gas pressure, in. Hg
Tr
-..1@!-=
absolute stack temperature, oR
Qs_L.@_= dscfm
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TECHNICAL {} NOU!)
Appendix A
Example Calculations
Location:
Source:
Project No.:
Run No.:
Parameter:
Rio Tinto Kennecott - Magna, UT
Flash Smeltins Furnace Drv Feed Bin Bashouse SME005
AST-2023-3179
PM
Dry Gas Meter Calibration Check (Yqa), dimensionless
Y-
Yqa =
where,
Y 1.05 = meter correction factor, dimensionless
O 60 = run time, min.
v'-.E= total meter volume' dcf
T, _;!@!-= absolute meter temperature, oR
^H@g=orificemetercalibrationcoefficient,in.H2oPb@= barometric pressure, in. Hg
AHa,g4=averagepressuredifferentialoforifice,inH2o
Md ....A= molecular weight (DRY)' lb/lb mol
(^H),,,4=averagesquaIerootpressuredifferentialoforifice,(in.H2o)1/2
Yqu4=percent
Volume of Nozzle (Vn), ft3
(*
**)
x 100
Ts/
Vn = F; ( 0.002669 xVlc *
where,
Vm x PmxY
Trn
Ts 623.8 = absolute stack temperature, oR
Ps 26.91 = absolute stack gas pressure, in. Hg
vt.TF= volume of H2o collected, ml
Vm 39.076 = meter volume, cf
P^ &= absolute meter pressure, in. Hg
Y 1.050 = meter correction factor, unitless
Tm 567.1 = absolute meter temperature, T.
Vn 46.212 = volume of nozzle, ft3
Isokinetic Sampling Rate (I), 7o
r=(
where,
)*roo
Vn
0x60xAnxYs
46.212 = nozzle volume, ft3
60.0
0.00052
24.1
10 1.7
Filterable PM Concentration (C,), grain/dscf
Mn x 0.0154
= run time, minutes
= area of nozzle, ft2
= average velocity, fl:/sec
=%
= filterable PM mass, mg
= standard meter volume, dscf
= grain/dscf
Vn
0
An
Vs
I
cr=
where,
Vmstd
Mn
Vmstd
c.
5.5
34.403
0.002s
0.0319xTmx29
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Location: Rio Tinto Kennecott - Magna, UT
Appendix A
Example Calculations
Source: Flash Smeltins Furnace Drv Feed Bin Baghouse SME005
Project No.: AST-2023-3119
Run No.: 1
Parameter: PM
Filterable PM Emission Rate (PMR), Ib/hr
C"xQsx60DIlitD
-
-:-
7.0E + 03
where,
C,--.,1!fu= filterable PM concentration, grain/dscf
Qs 1,796 : average stack gas flow at standard conditions, dscfm
PMR 0.038 = lb/hr
Condensable PM Concentration (C6py), grain/dscf
Mcpu X 0.0154Ccpu=fr
where,
Mcrr[= condensable PM mass, mg
Vmstd _lli!03 = standard meter volume, dscfC.rr;!fu= grain/dscf
Condensable PM Emission Rate (ER6py), Ib/hr
Ccpvr x Qsx6}fl*- 7nF:+ 03
where,
C.r, _;![ = condensable PM concentration, grain/dscf
Qs _L,7%_ = avera,ge stack gas flow at standard conditions, dscfm
ER.or;![-=lba,
Total PM Concentration (C1py), grain/dscf
Crpv=Cs+CcpM
where,
C.;!Q![= filterable PM concentration, grairVdscf
Ccr, 0.0035 = condensable PM concentration, grain/dscf
CrpM 0.0060 = grain/dscf
Totrl PM Emission Rate (ER1py), lb/hr
ERrpu=PMR+ERcpM
where,
PMR.................!L= filterable PM emissionrate, lb/hr
ERcrrA= condensable PM emission rate, lb/lrr
ERrpv 0.0049 = lb/hr
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TEfiHh} iO&L fiT{(.JL.!1"1
Emission Calculations
Location Rio Tinto Kennecott - Magna. UT
Source Flash Smelting Furnace Dry Feed Bin Baghouse SME005
Project No. AST-2023-3r79
Parameter PM
lun Number Runl Run2 Run3 Averase
)ate
Itart Time
Jtop Time
lun Time. min (e)
10125123
11: l4
12:20
60.0
10125t23
14:40
1 5:48
60.0
10t25t23
17:44
I 8:02
60.0 60.0
INPUT DATA
larometric Pressure, in. Hg
ltleter Correction Factor
f rifi ce Calibration Value
VIeter Volume, ft3
Vleter Temperature. oF
Vleter Temperafure, oR
Vleter Orifice Pressure. in. WC
Volume H2O Collected, mL
tlozzle Diameter, in
{.rea of Nozzle. ft2
rilterable PM Mass, mg
londensable PM Mass, mg
\{easured PM1 0 Fraction
rilterable PM10 Mass, mg
(Pb)
(Y)
(^H @)
(vm)
(Tm)
(Tm)
(AH)
(V1c)
(Dn)
(An)
(Mn)
(Mcpr'a)
(Mr*,n)
26.88
1.05
1.685
39.076
107.5
567.1
1. 133
16.2
0.310
0.0005
5.5
7.9
12.90
0.7r
26.88
1.05
1.685
43.053
115.0
574.6
1.371
16.7
0.3r0
0.0005
9.5
2.0
13.50
1.28
26.88
1.05
1.685
44.283
1 15.4
575.0
1.450
15.7
0.31 0
0.0005
4.1
1.9
14.20
0.58
26.88
1.05
1.685
42.137
1t2.6
s72.3
1.318
16.2
0.310
0.0005
6.4
3.9
I 3.5
0.9
ISOKINETIC DATA
itandard Meter Volume. ft'
itandard Water Volume, ft3
VIoisture Fraction Measured
\tloisture Fraction @ Saturation
Vloisture Fraction
Vleter Pressure, in Hg
Volume at Nozzle. ft3
sokinetic Sampling Rate, (7o)
)GM Calibration Check Value, (+/- 5%o)
(Vmstd)
(Vwstd)
(BWSmsd)
(BWSsat)
(Bws)
(Pm)
(Vn)
0)
(Y.,)
34.403
0.764
0.022
0.390
0.022
26.96
46.212
101.7
1.6
37.434
0.788
0.021
0.389
0.021
26.98
50.212
102.3
1.3
3 8.483
0.740
0.019
0.407
0.019
26.99
51.691
100.9
1.3
36.773
0.764
0.020
0.39s
0.020
26.98
49.37
101.6
t.4
EMISSION CALCULATIONS
ilterable PM Concentration, grain/dscf
ilterable PM Emission Rate. lb/hr
(c.)
(PMR)
0.0025
0.038
0.0039
0.065
0.0016
0.029
0.0027
0.044
londensable PM Concentration, grain/dscf
londensable PM Emission Rate, lb/hr
(Ccpr,r)
(ER"or)
0.0035
0.055
0.00082
0.014
0.00076
0.0 13
0.0017
0.027
rilterable PMI 0 Concentration, grair/dscf
lilterable PM10 Emission Rate. lb/hr
(Cpu,)
(ER"-')
0.00032
0.0049
0.00053
0.0088
0.00023
0.0041
0.00036
0.0059
l8 of80
nllmrps
TEC'.{Ni(;AL fiNQUP
Emission Calculations
Location Rio Tinto Kennecott - Magna, UT
Source Flmh S-"ltjng Fr.nu." Dry F""d
Project No.
Parameter PM
Run Number Runl Run2 Run3 Averase
Date
Start Time
Stop Time
Run Time. min
1012s123
1 1:14
l2:20
60.0
1012st23 10t25t23
14:40 17:44
15:48 18:02
60.0 60.0 60.0
VELOCITY HEAD, in. WC
Point 1
Point 2
Point 3
Point 4
Point 5
Point 6
Point 7
Point 8
Point 9
Point 10
Point 11
Point 12
Point 13
Point 14
Point 15
Point 16
Point 17
Point 18
Point 19
Point 20
Point 21
Point22
Point 23
Point24
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
6
4
5
5
4
6
5
4
2
J
2
1
6
5
6
4
5
4
J
4
J
J
2
2
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
l4
l6
t8
10
t9
t8
t8
l7
l7
t8
l0
l7
LI
t8
t6
l7
t5
t4
t6
t5
t4
l2
t3
t2
0.15
0.17
0.20
0.1 5
0.22
0.1 8
0.15
0.19
0.24
0.17
0.14
0. l6
0.18
0.17
0.21
0. l6
0.19
0.22
0.18
0.15
0.17
0.20
0.16
0.14
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
5
6
8
7
8
7
6
7
8
6
5
5
7
7
8
6
6
7
6
5
5
5
4
J
CALCULATED DATA
Square Root of AP, (in. WC)"-
Pitot Tube Coefficient
Barometric Pressure, in. Hg
Static Pressure, in. WC
Stack Pressure, in. Hg
Stack Cross-sectional Area, ft'
Temperature, oF
Temperature, oR
Moisture Fraction Measured
Moisture Fraction @ Saturation
Moisture Fraction
02 Concentration, o%
CO2 Concentration, o/o
Molecular Weight, lb/lb-mole (dry)
Molecular Weight, lbilb-mole (wet)
Velociw. ftlsec
(^P)
(cp)
(Pb)
(Pe)
(Ps)
(As)
(r0
(rs)
(BWSmsd)
(BWSsat)
(Bws)
(o,
(co,
(Md)
(Ms)
(Vs)
0.373
0.840
26.88
0.46
26.91
1.67
164.1
623.8
0.022
0.390
0.022
20.9
0.1
28.85
28.62
24.1
0.403
0.840
26.88
0.46
26.91
1.67
163.9
623.6
0.021
0.389
0.021
20.9
0.1
28.85
28.63
26.0
0.420
0.840
26.88
0.46
26.91
r.67
165.9
625.5
0.019
0.407
0.019
20.9
0.1
28.85
28.65
27.1
0.398
0.840
26.88
0.46
26.91
1.67
164.6
624.3
0.020
0.395
0.020
20.90
0.1 0
28.85
28.63
25.7
VOLUMETRIC FLOW RATE
A.t Stack Conditions, acfin
A.t Standard Conditions, scfm
4.t Standard Conditions, dscfm
(Qa)
(Qsw)
(Qs)
2,413
r,836
1,796
2,607
1,984
t,943
2,721
2,064
2,026
2,s80
1,962
1,922
l9 of80
Al6rce
TENP{NICAL fififJI,P
Method 1 Data
Locdion Rio Tinto Konecotr -UT
Source Flssh Smelting Fumace Fed
Prcjet No. AST-2023-3179
Dilet lol24l23
DuctOricntdion: Vdical
D,ct Dsignr-.Iilii-
Dilrmcc from Ftrr wtrll ro outri.t" of Pon,.......ffiin
Nipplc trngthr-766-in
Depth of Drc' ---i-3i- in
Cro3s sstionel Area of Dr.tr ---iii- 6'
No. ofTc$t Pofi!: 2
Di.tnna er---lij-ft
Distmc€ A Dud Diomderr,---lif-(mrsr be z 0.5)
Distme B: 5.0 ft
Disbe B Dud Diomte.s,--Ti-(.r.t b" > 2)
Minimum Number ofTrlverse Point: 24
Acuat Number of Trav"r." Pointr, ----fi-
Number of Reading* pe, Point,--j--
Mecurcr (Initiot md Dile)x JS!!IZ!!E-
Rei@er (ltriti&l ud Datett'l [Ll l0D4l23
LOCATION OF TRAVf,RSE POTNTS
Numba of tnvae poinls on d didMa
I
3
4
5
6
1
8
9
l0
il
t2
a 3 1 6 1 I 9 t0 ll l2
t4.6
85.4
6.7
25.0
75.0
,:-,
4.4
t4.6
29.6
70.4
85.4
,r_,
3.2
10.5
19.4
32.3
67.7
80.6
89.5
96.8
2.6
8.2
14.6
22.6
34.2
65.8
77.4
85.4
91.8
'',.0
2.1
6.7
I 1.8
17.7
25.0
35.6
64.4
75.0
82.3
88.2
93.3
97.9
diomeler ftom insicle
Tnrene
Point
o/. ol
Dimder
Distmce lrom
outsidc of$trll
I
3
4
5
6
1
8
9
l0
ll
t2
2.t
6.7
il.8
17.7
25.0
35.6
64.4
75.0
82.3
88.2
93.3
975
0.50
l.l7
2.07
3. l0
4.38
6.23
|.27
t3. t3
14.40
15.44
16.33
t700
7 t/2
8 3/16
I t/t6
l0 l,a
lt 3/8
13 1/4
t8 l/4
20 l/8
zt 318
22 7^6
23 5fi6
)4
tHoffi'0.6! m(?tr^.)
Stack Diagmm
A = 26.5 ft.
B=5ft.
DepO of Duct = I 7.5 in.
Cross Selional Afta
o
o
a
a
a
aa a a o o a a oa
o
o
a
o
a
Disturbance
20 of 80
anIffirme
IEfiHI,II$AL (IfiOL.I i}
Cyclonic Flow Check
Location Rio Tinto Kennecott - Magna, UT
Source Flash Smelting Furnace Dry Feed Bin Baghouse SME005
Project No. AST-2023-3179
Date 10/24123
Sample Point Angle (AP=O)
1
a
3
4
5
6
7
8
9
l0
11
t2
13
t4
15
t6
t7
18
t9
20
2t
22
23
24
Average I
2l of80
ntlffinsg
rEU-IhII$AL GfiOL} i:N
Method 4 Data
Location Rio Tinto Kennecott - Magna, UT
Source Flash Smelting Furnace Dry tr'eed Bin Baghouse SME005
Project No. AST-2023-3179
Parameter PM
Analysis Gravimetric
Run I Date:t0125/23
Impinger No.1 a 3 4 Total
Contents Empty Erpty H20 Silica
Initial Mass, g 482.9 640.2 712.3 949.6 278s.0
Final Mass, g 488.0 641.4 711.8 960.0 2801.2
Gain 5.1 t.2 -0.5 10.4 t6.2
Run 2 Date:10125/23
Impinger No.I 2 3 4 Total
Contents Empty Empty H20 Silica
Initial Mass, g 498.7 631.9 746.3 954.0 2830.9
Final Mass, g 503.7 633.8 746.6 963.5 2847.6
Gain 5.0 t.9 0.3 9.s 16.7
Run 3 Date:10125123
Impinger No I 2 3 4 Total
EmpE EmpB It2o Silica
Initial Mass, g 482.5 640.6 71 1.8 960.0 2794.9
Final Mass, g 488.8 640.8 712.0 969.0 281 0.6
Gain 6.3 0.2 0.2 9.0 15.7
22 of80
Isokinetic Field DataI t_ c 1t N i cA i.,. G l:i r_] L.i ;:
Localion: Rio Tinlo Kennecott - Magna, UToot"rffi Start Time:
End Time:
11: l4
12t20
Solrce: Flash Smelting Furaace Drv Feed Bin
ProjectNo.: AST-2023-3179 | Parameter: PM
STACK DATA (EST}EOIlIPMENT S'I'A(]K T)A'I'A
'ESTI
FILTER NO.STACK DATA (FINAI,)MOIST. DATA
Moisttrre: 2, 7o est.
Barometric: 26,88 in. Hg
Static Press: 0.46 in. WC
Stack Press: 26.91 in. Hg
CO2: M ok
o2: 2A6 o/o
NICO: 793 %
Md: 28.84 lb/lb-mole
Ms: 28.60 lb/lb-mole
Meter Box ID: MB-30
Y: 1.05
au@(in.wc),lJc-F-
Probe ID: 3179-l
Liner Material: glm
Pitot ID: 31 79-l
Ritot Cprryp",ilh-fffi
No,,t" to' lJilll--T-Illf
Nozle Dn (in.): 0.310
Est. Tm: 140 'F
Est. Ts: 144 'F
Est. AP: 0.13 in. WC
Est. Dn: 0.299 in.
,ai Dol6. n (< "^f-
t6749-C Pb: 26.88 in. Hg
Pg: 0.46 in. WC
Or: 2O-g o/.
CO2: 0.1 %l--iffii
Mc (ml)
16.2
K-FACTOR
4.872
Final Corr.
LEAK CHECKI Pre Mid I Mid 2 Mid 3 Post o r0r.217 101.304
Mid 2 (cl)
Mid 3 (cD
Leik Rate (cffr): 0.000 0.000 0.000
Vacuum (in Hg): l5 5 -- - 5
Pitot Tube: Pass Pass Pass i{id-Point Leak Check Vol (cD:
o
=.bL
Sample Time
(minutes)
Dry Gas Meter
Reading
(ft3)
Pitot
Tube
AP
(in wC)
Uas IemDeratures Orifice Press.
AH
(in. WC)
Pump
Vac
(in. Hg)
(irs'l
% lso Vs
(rps)
DGMAT Stack Probe Filter Exit Aux
Beein End Idesl Acftrrl
AI 000 250 81 838 0 t6 I01 164 )9 30 2 244 266 62 83 100.6 25.86
2 250 500 i 54'l 0 101 163 l3 l0 2 256 265 59 82 101.5 24.17
500 7.50 85.162 0 101 165 20 20 2 248 255 58 80 t0t 3 25.05
4 750 10 00 86.827 0.102 t10 20 20 2 254 251 57 80 t0l 9 25.15
5 t0.00 12.50 88.498 0.102 161 l3 t0 2 252 254 58 7A 103 3 24 13
6 12.50 15.00 90 147 0 6 r02 160 30 130 2 ?.5i 249 60 78 101.0 25.71
7 r5 00 1750 9t 871 0 5 t04 161 ).o 248 248 62 79 101 8 25.09
8 150 20 00 93 551 0 105 158 l.t5 1.10 2 258 250 62 79 100.5 24.07
9 20.00 22.50 95.168 0.106 156 0.99 1.00 2 247 250 62 80 10 4
t0 22.50 25 00 96.684 0 r07 164 1.06 1.00 258 249 6l 8l 21 11
t1 25.00 2'1.50 98.261 0.2 107 166 097 099 2 245 244 5 22.43
12 21 50 30 00 99.169 0lt 108 163 090 og )s5 ?5i 60 80 .4
B1 30 00 32 50 t0t 2t7 0 t6 108 15)'lo 243 247 6t 8l 105.0 25.81
32 50 500 103 I1 0 tos 166 22 20 2 251 252 60 8l 101.6 25.07
35 00 750 I 04 80d 0 109 16'1 30 30 2 244 251 6l a2 I0t 7 25.92
4 ?7 S0 40 00 106 551 0.109 169 t3 l0 2 247 250 6l 101 0
5 40.00 42.50 t08.r72 0.l0 169 22 20 2 252 60 100 4 25 t3
6 42.50 45.00 109.843 0 158 16 20 2.24i ).51 83 102.0 24.07
7 45 00 47 50 ) 501 0 r63 01 242 248 6 83 99.6 23.29
8 47 50 50 00 3 057 0 167 l.l4 20 259 251 6 83 102.3 24.24
9 50 00 52 50 4.710 0 16'1 1.06 l0 2 240 252 84 100 I 23.36
l0 52.50 55.00 6.285 0 164 l .07 t0 2 245 252 62 84 100 4 23 31
ll 55.00 57.50 7.858 0 2 3 164 099 00 259 250 62 R4 t0l 2239
12 5? 50 60 00 9.381 o 3 165 0.98 00 255 256 62 84 t02 0 22.41
1 Final DGM: 20.9t4
aFrtpa
RunTime Vm AP Tm rs U: ^H %rso Bws Y."
60.0 mrn 39-076 ft3 0.14 in. WC 107.5 164.1 1.133 in.WC 101.7 0.022 I.6
23 of 80
.ffi
TTCIII'JiCAL GFCLI N Isokinetic Field Data
Loc{tion: Rio Tinto Kennecotl - Maqna, UTOot",ffi Start Time: 14:40
f,lnd Time: 15;48
Source:
Project No.;
FIash Smeltins Furnace Dry Feed Bin
AST-2023-3179 I Prrnmeter: PM
STACK DATA (EST)EQUIPMf,NT STACK DATA (EST)FILTER NO. S1-ACK DATA (FINAL)MOIST. DATA
Moisture: 2J 7o est.
Barometric: 26.88 in. Hg
Static Press: 0.46 in. WC
Stack Press: 26.91 in. Hg
CO1: 0J %
O2t 2U6 o/o
NIICO: 793 Yo
Md: 28.84 lb/lb-mole
Ms: 28.61 lb/lb-mole
Meter Box ID: MB-30Y'L-
AH @ (in.WC): 1.685
Probe ID: 3l 79-l
Lin." Mot.riol' !GI-
Pitot ID: 3179-1
Ritot Cp,"ryp", ildfi-JffiN*rt"tO,@
Nozle Dn (in.): 0.310
Est. Tm: t07 'F
Est. Ts: 161
Est. AP: 0.14 in. WC
Est, Dn: 0,305 in.
Tarset Rate: 0,65 scfm
t6170-C Pb: 26.88 in. Hg
Pg: 0.46 in. WC
Or: 20.9 %
CO2: 0.1 %lffiFt. r"rtr"-i
16,7
K-FACTOR
8.1 4
Final Corr
,EAK CHECK! Pre Mid I Mid 2 Mid 3 Post Mid 1 (cf) 143.287 143.131,
Mid 2 (cf)
Mid 3 (cf)
L€flk RAre (cfm)i 0.000
Vacuum (in Hg): 15
Pitot Tube: Pass 4id-Point Leak Check vol (c0:
Sample Time
(minutes)
Dry Gas Meter
Reading
(ft3)
Pitot
Tube
AP
(in wC)
Gas TemDeratures ("F)Orifice Press.
AH
(in.wC)
Pump
Vac
(in. Hg)
% rsc Vs
(fps)
DGM Average Stack Filtcr Imn tr'.rif
Beein End Ideal Actual
AI 000 250 r 21 201 014 108 62 l5 20 2 248 249 65 84 101.3 24.14
250 500 t22 434 016 108 65 30 130 2 255 248 63 82 103.4 25.81
500 750 124 612 018 108 46 50 3 252 250 62 80 r00 6 2',7.51
4 '1.50 r0.00 126.441 0.20 0 64 64 1o ?49 64 80 07.2 28 90
5 10.00 12.50 128.412 0.19 66 55 60 3 251 65 80 I 03.1
6 12 50 15 00 130 351 0 8 2 59 49 50 3 256 250 65 8t 100.5 2'1.31
7 t5 00 17 50 ]12204 0 18 113 62 49 50 3 254 251 66 82 l0l 3 27.37
t7 50 20 00 134 011 0 1 3 65 40 40 3 250 66 81 I00 I 26.67
9 20.00 22.50 5.861 0 7 4 63 40 40 24i 250 66 80 oo9 26.62
t0 22.50 25.00 t37.671 0 8 4 67 48 50 259 )4R 19 t 0l i 21 48
ll 25.00 27.50 139.534 0.20 4 65 64 70 3 253 249 64 '79 99.9 2a 92
12 21 50 30.00 l4l,.413 0.17 5 59 4l .40 3 243 250 64 78 t00.6 26.54
Fll 30 00 32 50 143 287 011 il5 62 41 .40 3 240 251 63 995 26.60
250 i5 00 145 52 0 t8 7 66 49 50 3 254 248 62 't9 to22 2'1.46
3 15.00 37.50 147.412 0. l6 7 5g t34 40 252 250 62 80 I00 fi 2515
4 3"1.50 40.00 149. I 78 0.1 7 63 4t 40 3 25t 25 62 8l t0t.4 26.62
5 40.00 42.50 51.007 0 5 8 65 )A 30 3 248 25 6t 79 t0l .3 25.05
6 42 50 45 00 0 4 8 63 16 20 250 25 6l 80 102.9 24.t6
1 45 00 47 50 54 412 0 t6 119 60 14 40 3 251 25 6l 80 t000 25.'7',|
8 4't 50 50 00 56 17?s 9 61 24 30 3 252 250 6l 80 t009 25.09
9 50.00 52.50 57 88 4 I 55 t6 )o 744 ?5?5)91 101 5 24 20
t0 52.50 55.00 59.547 0.2 20 t66 00 .00 3 250 254 62 84 t02.3
ll 55.00 57.50 161. I 02 0 3 20 r68 08 l0 3 248 246 64 84 101.9 2334
l2 57.50 60.00 t62.7t2 0 2 20 165 00 oo 3 247 245 65 83 101.3 22.4)
Final DGM 164.254
a
Fa
rrl
Run Time Vil AP Tm Ts Yo' AH %ISo Bws Yru
Vac
60.0 mrn 43.053 ftr 0.16 in. WC 1 15.0 163.9 3 1-371 in. WC 102.3 0.021 1.3
24 of 80
#AIlarrce"].TC!INiCAL GNTJL] :}Isokinetic Field Data
Location: Rio Tinto Kennecott - Magna, UTOar",@ Start Time:
End Time:
Source: Flash Smelting Furnace Dry Feed Bin Baghouse SI
""0j"","o,,@
STACK DATA (EST)EOUTPMENT STACK DATA (EST)FILTER NO.STACK DATA (FINAL)MOIST. DATA
Moisture
Barometric
Static Press
Stack Press
Coz
o2
N2/CO
Md
Ms
2-2 o/o est
@tn us
0.46 in WC
l?Fin ug
L%
L%
_J2t_%
28.84 lb/lb-mole
28.60 lb/lb-mole
Meter Box lD: MB-30,,.![
AH @ (in.WC)r 1,685
Probe ID: 3179-1
Liner Material: glN
Pirot IDi 3179-1
Pitot cp/ryp", ili76-Jffi
Norrl"IDr@
Nozzle Dn (in.): 0.310
Est- Tm: I l5
Est. Ts: 164 "F
Est. AP: 0.16 in. WC
Est. Dn: 0.291 in.
Tarset Rate: 0.65 scfm
1611L-C 26.88 in. Hg
0.46 in. WC
L%0.1 v.
I Check Pt. Initial
Pbl
Pg:
or:
CO2:
Vlc (ml)
15-7
K-FACTOR
8.235
Final Corr.
-EAK CHECKI Pre Mid 1 Mid 2 Mid 3 Post Mid I (cf) 186.614186.961
Mid 2 (cD
Mid 3 (c0
Leak R{te (cfm): 0.000 0.000 0.000
Vacuum (in Hg)i 15 5 -- -- 5
Pitot Tube: Pass Pass Pnss {id-Point Leak Check Vol (c0:
d9au
Ssmple Time
(minutes)
Dry Gss Meter
Reading
(ft')
Pitot
Tube
AP
(in wC)
Gas Temneratures (oF)Orifice Press.
AH
(in. wC)
Pump
Vac
(iu. Hg)
Gas TemDeratures (oF)
% ISC
Vs
(fps)
DGM Averase Stack Probe Filter lmn Exit Aur
Besin End Ideal Actual
000 2SO 164 558 0 r5 62 20 2 251 255 65 75 998 24.',l4
2 5C)500 166214 o 1'1 ]]l 170 I 4l 40 241 249 5 7 105 I 27 09
500 '7 50 58 I t4 o?o 68 50 259 250 54 76 1o2.9 29 00
4 7.50 r0.00 70.094 0.15 68 20 2 246 245 53 '14 l0 t.l 25.1 1
5 10.00 12.50 1."182 or)72 78 80 3 245 52 73 l 00.9 30.51
6 12.50 I 5.00 3.8r 0.1 8 53 50 50 )255 252 52 72 t00 6 27.la
7 r500 17 50 5 671 015 2 53 25 30 2 248 251 52 73 99'1 24.81
8 17 50 20 00 I 77 358 019 113 52 159 60 3 244 252 s2 74 0r0 27 90
9 20.00 22.50 79.284 0 4 1 52 0l 00 3 246 253 53 75 I01.7 31.36
t0 25.00 81.461 0 1 3 55 42 40 3 251 25t 53 "15 r00.3 26.46
ll 25 00 27.50 83.267 0 4 3 5l 1't 20 2 252 25r 53 76 99.8 23.93
12 2'.7 50 30.00 84.904 0 6 4 60 .33 .30 3 257 250 54 7't IOI 5 25.'77
BI l0 00 :12 50 I 86 674 0 8 4 63 48 50 3 259 253 71 t0l 3 27 40
32 50 35 00 t88 541 0 1 8 73 3S 40 3 241 249 80 996 26 a4
500 37 50 90 1)4 0 70 7)70 24'1 5 79 100.4 29.76
4 37.50 40.00 192324 0.16 8 65 32 30 3 256 256 55 7'l 101.7 25.88
5 40.00 42.50 t94.102 0.19 9 72 56 50 3 250 248 55 1',|r02.9 28.36
6 42 50 45 00 196.054 022 9 73 80 80 3 245 248 56 7a I0t 4 30.54
1 45 00 47 50 r98 120 0t 9 74 4't 50 3 244 a1 78 ool 27 64
4'7 50 50 00 I gg 965 0t 9 74 )o )4))50 a1 19 o1 I 25 23
9 50 00 s? 50 )o1 561 0 r7 )n 7 'lc)40 250 58 '78 100.6 26.89
t0 52.50 55.00 203.472 nro 20 175 .63 60 3 248 250 55 7't l0l.l 29.t6
tl 55.00 57.50 205.43'1 0.16 20 r75 3l 30 3 253 254 55 76 t00.8 26.08
t2 57.50 60.00 207.192 0. l4 t76 14 l0 3 257 252 55 76 t01.1 24.42
Final DGM: 208.841
aF
FlD0
RunTime Vm AP Tm Ts Y"" AH %rso Bws Yoo
Vac
60.0 mrn 44_243 ft'0.18 in. WC 115.4 0F 165.9 0F 3 1.450 in. WC 100.9 0.019 1.3
25 of 80
26 of80
Allionce Technicol Group, LLC
Anolyticol Services
5530 Morsholl St.
Arvodo, CO 80002
(720) 4s7-e s04
www.ollioncetg.com
Anolyticol Loborotory Report
Rio Tinto Kennecott
4Z0O Doybreok Porkwoy
South Jordon, UT 84095
Project No. AST-2023-31 79
27 of80
1 of21
Certificotion Stotement
Allionce Source Tesling, LLC (AST) hos completed ihe onolysis os described in this report.
Results opply only to the source(s) tested ond operoiing condition(s) for the specific test
dote(s) ond time(s) identified within this report. All results ore inlended to be considered in their
enlirety. ond AST is not responsible for use of less thon the complete test report without wriiien
consent. This reporl sholl not be reproduced in full or in porl without wriilen opprovol from lhe
customer.
To the best of my knowledge ond obilities, oll informotion, focts ond test doto ore correct.
Doto presented in this report hos been checked for completeness ond is occurote. enor-free
ond legible. Any devioiions or problems ore detoiled in the relevoni sections on the test report.
This document wos prepored in portoble document formot (.pdf) ond contoins poges os
identified in the botiom footer of this document.
Volidotion Signoture
The onolyticol doio ond oll QC contoined within this report wos reviewed ond volidoted by
the following individuol.
James Davidson
Jomes Dovidson
Quolity Assuronce Associole
Digitelly signed by Jsmes Davidson
ON: C=US, CN=James Davidson, E=james.davidson@stacklest.@m
Rasn: I attest lo thc 8@uEc1 and integrity of this document
Loelion: your signing lo@tion here
Dalei 2023.1'1.28 21:59:47-06 00'
Foxit PDF EditorVeBion: 11.2.7
Dote
28 of80
2of21
Proiecl Norroiive
Anolyticol Method(s):
Method 5 - Determinotion of Porticulole Motier Emisslons From Stoiionory Sources
Method 202 - Dry lmpinger Method for Determining Condensoble Porticuloie Motter
Emissions From Stotionory Sources
Filteroble The filter(s) were eiiher oven dried ond/or desiccoted per ihe melhod until o finol
weight wos obioined. The liquid froctions were extrocted if required, evoporoted ond
cooled until o finol weight wos obtoined. These frociions were summed together to
provide the totol Porticulote Motter collected.
Condensoble The filter(s) were extrocted per ihe meihod. The orgonic extroct wos odded io the
orgonic rinse, ond the inorgonic extrocl wos odded io the inorgonic rinse. The
inorgonic froction wos extrocted wiih solveni per the method. Extrocts were combined
with the orgonic rinse. The orgonic ond inorgonic froctions were evoporoted ond
desiccoted until o finol weight wos obtoined.
MDL The Minimum Detection Level (MDL) is 0.5 mg per froction. lf the meosured resull for o
froction is less thon the MDL, the MDL wos used in ensuing colculotions.
Blonk Correction lf blonk correction is performed, only blonk volues returned higher thon ihe MDL ore
used. lf o blonk returns o volue less thon the MDL, no correction is included.
Custody: The somples were received by Cory Monshock on I I/l 4l23in Arvodo, CO. The
somples were received in good condition wiih proper Choin-of-Custody
documentotion. No opporent contoiner problems were noted upon receipi. Prior to
onolysis, the somples were kept secure with occess limited to outhorized personnel of
AST.
Number of Somples: 23 (2 On Hold)
Lobeling: Acceptoble
Anolyst: Cory Monshock - Loborotory Anolyst ll
Corson Williomson - Loborotory Anolyst I
Ryon Gillett - Loborotory Anolyst ll
Eric Grosjeon - Technicol Director
Equipment: Mettler Toledo Bolonce ML-104, SN 82l 7893065. This scole wos used for onolyticol
determinotions of filters ond rinse vessels.
Denver lnstruments Bolonce T8-6201, SN ,l7904189. This scole wos used to meosure ihe
totol moss of rinse collected for blonk correction.
Anolysis wos performed on the some bolonce qs ihe ossocioted tore.
Quincy Lob lnc oven, 30CG, SN G3-012673.
Lob Reogents: Acetone Lot Number: 224521
Hexone Lot Number: 216612
QC Notes: The somples met ihe minimum criterio estoblished by the relevonl method.
A blonk correction wos opplied per lhe meihod.
Reporting Notes: none
29 of 80
3of21
City, Stote
Projecl No.
Melhod
GROLJP
lio Ilnlo Kennecoll
outh Jordon. Ln 84095
\sT-r02331 79
:PA Method 5
troni Hqlt Fller
lob lE D3831 6 D38321 D38326
Fleld lt M5/202 - SME005 - Run I Cont. I M5/202 - SME005 - Run 2 Conl. l M5/202 - SME005 - Run 3 Conl. l
Fllter lE 16749 - C 16770 -C 1677t -C
Flller Tqre Welghl, e 4.47&0.4846 0.4701
Dole - Deslccolor | | lt 4/23 t1 /14123 11 /1 4123
nme - Deslccolor l0:40 l0:40 10:{0
Doie of WelghlnC 1 1 /1 5/23 t1 /16/23 11t15t23 l1 A 6t23 t1/151?11 /1 6123
Tlme of Welghlne ,tl2 12137 5t2 l2:37
Flller Welght, e o.4777 o.4776 0.4895 0.4896 o.4721 4.4720
Rller PM Mo$, mg*1.7 5.0 2.0
tronl Holt Rln3e
Iob lE D383r 7 D38322 D38327
tield lt M5/202 - SME005 - Run I Cont. 2 M5/202 - SME005 - Run 2 Cont. 2 M5/202 - SME005 - Run 3 Conl. 2
Beoker ll 32A60 32468 32479
8eqker lqre, r 3.9066 3.8942 3.8622
Beoker wllh Acelone, !72.7 84.4 63.3
Acelone Mqs3, !68.8 80.s 59.4
Dole . Deslccolo 1t 114/23 t1/14/X 1t 114/23
IIme - De.lccdlor 14:00 l4:m l4:00
Dqle ot Welghln€1 | t1 5/23 t1 /16/23 | 1 / 15/23 11 /16/23 t1 11 5/23 t I /l 6t23
nme o, welghlnc I 4146 5:17 I 4:46 5:17 | 4:46 5:l 7
Walght, C 3.9r 05 3.9rm 3.4987 3.8985 3.8644 3.8642
Meqsured Rin3e Mq!!, mg 3.8 4.5 2.2
Blonk Conectec No
Iotol PM Ms!, me 5.5 9.5 4.1
'All froclions were onolyzed ond relurned volues greoter lhon the MDL of 0.5 mg.
30 of80
4ot21
Ctty,Slolc
lio llhlo Kennecolt
buth lordon. uT84095
\sl-2023-3r 79
Acelom Blonk
tob lI D3833r
tl.ld ll MS Acelone Blonk
Beoks lt 324s8
B6ker lorc, !3.9049
Beoker wllh Acclone, !74.70
Acelona Mca, e 704
Dolc - Dslccolo 11 /14/23
Ilme . De3lccolo t40o
Dole ol Welghln(1 1 /1 5/23 1t/rc/a
IImc o, welghln(1 4:46 5il7
W.lelrt, (3.9054 3.90s2
Bldnk M$i, mg'0.0
3l of80
5of21
EAlia.TECHNICAL
CiV, Sl,ote
Prorecl No.
Melhod
GROUP
?io Tinto Kennecoti
iouih lor.ion llT44095
AST-,O?3.31 79
EPA Method 202
Teion tlllral
tob lD D383r 8 D38323 D38328
tleld lD M5/202- SME005- Run I Cont. 3 M5/202 - SMEmS - Run 2 Conl. 3 M5/202 - SME005 - Run 3 Coni. 3
Orgonlc Froclion
lob lD D38320 D3&325 D38330
tleld l[M5/202 - SME005 - Run I Cont. 5 M5/202 - SME005 - Run 2 Cont. 5 M5/202 - SME005 - Run 3 Coni. 5
Beoker lI 32440 32463 32477
Baokei lole, g 3.&44 3.8973 3.8723
Beoker Solvenl, E 203.5 201.2 195.3
Solvenl Moss, !199.7 197.3 191.4
Dole . Desiccqlo 1 1 /14/23 t1 114/23 11 /14t23
nme . Deslccolo l8:00 l8:@ l8:00
Ddle ot Welghlnr 11 116/23 1 1 /17 123 11 t16t23 1l /16/23 11/ 16/23 11 /16/23
Ime ol welEhlnc I l:43 4:26 5:42 1 l:43 5:42 I l:43
Weight, g 3.8s23 3.8521 3.8987 3.899l 3.8752 3.8756
Orgonlc PM Moss, mg'7.8 1.6 3.1
lnorgonlc Frocllon
tob lD D3831 9 D38324 D38329
Field lD M5/202 - SME005 - Run I Conl. 4 M5/202 - SME@s - Run 2 Cont. 4 M5/202 - SME005 - Run 3 Conl. 4
Eeoker lD 3t550 31 570 31558
Beoker lore, q 70.9063 5r.3058 66.2608
Beoker Woler, q 409.2 330.9 419.6
Woter Mdss. q 338.3 279.6 SJ.J
Doie. Dcrlccolor t1 l1 4t23 t1 /14t23 t1 t14/23
Ilme - De3lccolor l8:02 l8:02 l8:02
Dolre ol lveighing t1 /16/B 11|6/23 11 /16/23 11 /16/23 11 /16123 t1 /16/23
nme o, WelEhlng I 1:49 5:47 I l:49 5'.47 1 1:49
welght, g 70.9082 70.9086 5 1.3080 5r.3084 66.2614 66.2618
Inorgonlc Moss, mg'2.1 2-t 0.8
Elonk Correcled
Tolol PM Moss, me 7.9 2.O t.9
"All froctions were onolfzed ond relurned volues greler thon ihe MDL of 0.5 mg.
32 of80
6of21
Clly,Stote
6HOUF ProJect No.
lio Tinlo Kennecott
;oulh lordon. uT84095
AsT-2023-3r 79
:PA Matho.J ,O?
I6llon tiller Elonkt
Fleld lroln Blonk Prool Blonk
[ob lt D38332
Fleld lt M202-FT Proof Recovery Blo.k Con'.3 N/A
Oroonlc troclion Blonks
fleld lroin Elonk Prool Blonk
lob lD D38334 D38336
Fleld lD M202-FT P'oof Recovery Blonk Conl.5 M2O2-FT Prool Blonk-Cont. 5
Beoker lD 32473 32481
Beqker tore, g 3.8922 3.8644
Bedker Solvenl, e 142.7
Solvenl Moss, g I 384 7).4
Dole - Deslccolor t) ll4l23 11/)4/23
Tlme. Deslccdtor l8:00 14i00
Dote of welghlng I I /l 6/23 | 1 /16/23 t t /t 5123 | 1 l1 6/23
Ilme ol WelghlnC ll:43 I 4:49 5:1 7
welght, e 3.8939 3.8937 3.8651 3.8649
Orgqnlc Moss, mg''t.6 0.6
lnorgonlc froctlon Elonks
fleld lroln Elonk Prool Blonk
Lob lI D38333 D38335
tleld lt M202-FT Proof Recovery Blonk Coni.4 M202-FT Proof BIonk-Cont. 4
Eeoker lE 3l 574 3t 564
Bedker tore, e 49.97 67 74.0239
Beoker woler !170.4
Woier Mqss, !172.4 96.4
Dole - Desiccolor | ) /14/23 t1 /)4/23
TIme - Deslccolor l8:02 l4:00
Dqle of Walghine ll /16t23 ) | /1 6/23 1 t /1 5123 t 1 116123
Ilme ol Welghln!5:47 I I:49 1 4:49 5:1 7
weight, (49.9744 49.9792 74.0236 74.0239
lnorgonlc Mdss, mg'2.0 0.5
33 of 80
7 of21
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34

of

80
Calibration Cefficate lD
NAI 548-038-030823-ACC-USL
MettlerToledo, LLC
'1900 Polaris Parkway
Columbus, OH 43240
1.80O.METTLER
Customer
lleEi6-nE'l
METTLER TOTEDO
Accredited by the American Association
for Laboratory Accreditation (A2LA)
CALIBRATION CERT #1 788.01
ISO 17025 Accredited
ANSYNCSL 2540-l Accredited
Accuracy Cali bration Certifi cate
Alliance Source Testing
5530 Marshall Sl
Company:
Address:
Clty:
Zip / Poshl:
Shte / Province:
Weighing Device
Arvada Conhc-t:Eric Grosiean
80002-3108
Colorado
ManufactJr€r:
Model:
Serial No.:
Buildirq:
Floor:
Room:
Mettler Toledo lnstumenl Type:
Asset Numb€E
Terminal Model:
Terminal Ssrbl No.:
Termlnal Asset No.:
Weighing lnstrument
l\ilL104103
B21 7893065
5520
Lab
1 120 g 0.0001 s
N/A
N/A
N/A
N/A
Procedurc
Galibraton Guideline:
METTLER TOLEDO Work lnstruc{on:
ASTM E898.20
30260953 v1.61
This calibration certificate including procedures and uncertainty estimation also complies with EURAMET cg-18 v 4.0.
This calibration certificate contains measurements for As Found and As Left calibrations.
The sensitivity/span of the weighing instrumenl was adjusted before As Left calibration with a built-in weight.
ln accordance with EURAMET cg-18 (1 1/201 5), the test loads were selected to reflect the specific use of the weighing device or to
accommodate specific calibration conditions.
As Found Start:21.1 'C End: 20.9'C Start: 21.0 % End:.21.0 %
As Left Start:20.8'C End: 20.7 "C Start:21.0 % End:20.0 %
Environmental conditions have been
verified to ensure the accuracy of the
calibration.
This certificate is issued in accordance with the conditions of accreditation granled by MLA, which is based on ISO/IEC 17025. A2LA
has assessed the measurement capability of the laboratory and its traceability to recognized national standards,
As Found Colibration Dab:
As Left Calibraton Date:
lssue Date:
08-Mar-2023
08-Mar-2023
08-Mar-2023
R€quosted N6xt Calibration Dab: 31-MaF2024
Authorlz€d A2lA SignatoM - ' -.-??r'''!
t"-:,.::'-' *'
Chris Carson
Software VeEion: 1.23.1.70
Report Vereion: 2.1 6.32
Fom Number: AF1702Lr1.0
O METTLER TOLEDO
This is an original document and may not be partially reproduced without the
written pemission of the issuing €libration laboratory.
Page '1 of 5
9 of21
35 of 80
Calibralion Cerliff cab lD
NA1 548-038-030823-ACC-USL METTLER TOTEDO Service
Measurement Results
Repeatability
Test Load: 100 g
100.0003 g 100.0001 s
2 100.0002 g 100.0000 g
J 100.0002 g 1 00.0000 g
4 100.0002 g 100.0000 s
5 100.0001 g 1 00.0001 g
100.0002 g 100.0000 g
7 100.0002 g 99.9999 g
8 100.0000 g '100.0001 g
9 100.0003 g 100.0001 g
'10 1 00.0002 s 100.0002 g
Standard;;il"; I 0.0000es i 0.00008s
Eccentricity
0 As Found
o As Left 1 (Tcsr Poinl)
>6d
'lo -. 4d
3d.
. 2d., .'. rc'a.a '^ O L)va na'V.O.. u Uo'.-..c_)o--
{i
The .d" in the graph represonts the roadability of the range/interual in which the
test was performed,
The results of this graph are based upon the absolute values of the differences
from the mean value.
Tost Load:50 g
Maxlmumffi;i;;J o.ooo1s | 0.0000s
The "d" in the graph represents the readability of the range/interval in which
tho tost was performed.
As Found As Lsft
Software VeEion: 1.23.1.70
Report Vecion: 2.16.32
Fom Number: AF1702Lr1.0
O I\IETTLER TOLEDO
This is an original document and may not be partially reproduced withoul the
written permission of the issuing @libration laboratory.
Page 2 of 5
10 of 21
36 of80
Calibration Certificab lD
NA1 548-038-030823-ACC-USL METTTER TOTEDO Service
Enor of lndication
As Found
1 N/A 0.0000 g 0.0000 g 0.0000 g 0.18 mg 2
N/A 20.0000 s 20.0002 g 0.0002 g 0.22m9 2
3 2og 20.0000 g 20.0002 g 0.0002 g 0.22m9 2
4 40g 20.0000 g 20.0001 g 0.0001 g 0.22m9 2
E 6og 20.0000 g 20.0001 g 0.0001 g 0.22 mg 2
80g 20.0000 g 20.0001 g 0.0001 s 0.22 mg
7 N/A 60.0000 g 60.0001 g 0.0001 g 0.35 mg 2
o N/A 100.0000 g 100.0003 g 0.0003 g 0.49 mg 2
I N/A 1 1 9.9999 s 120.0002 s 0.0003 g 0.59 mg 2
As L€ft
1 N/A 0.0000 g 0.0000 g 0.0000 g 0.18 mg 2
2 N/A 20.0000 g 20.0000 g 0.0000 g 0.20 mg
3 2og 20.0000 s 20.0000 g 0.0000 g 0.20 mg 2
4 4og 20.0000 s 20.0000 g 0.0000 g 0.20 mg 2
6og 20.0000 g 20.0000 g 0.0000 g 0.20 mg
b 8os 20.0000 g 20.0000 s 0.0000 g 0.20 mg 2
7 N/A 60.0000 s 60.0000 g 0.0000 g 0.24 mg 2
8 N/A 100.0000 g 100.0001 g 0.0001 g 0.27 mg 2
I N/A 1 19.9999 g 'r20.0001 g 0.0002 g 0.32 mg 2
F
C
.9
6.eE
o
o
r.u
0 As Found
C.5 a a AsL€fi
For improved legibility of the graphics
only increasing measurement points
are shown and measurement points
close to zero are not displayed.
1*
0
Calibralion Polnt8 lgl
The uncertainty stated is the expanded uncertainty at calibration obtained by multiplying the standard combined uncertainty by the
coverage factor k - which can be larger than 2 according to ASTM E898 and EURAMET cg-18. The value of the measurand lies within the
assigned range of values with a probability of approximately 95%.
The user is responsible for maintaining environmental conditions and the settings of the weighing instrument when it was calibrated.
Software VeEion: 1.23.'1.70
Report Ve6ion: 2.16.32
Fom Number: AF1702Lr1.0
O METTLER TOLEOO
This is an original document and may not be partially reproduced without the
written permission of the issuing €libralion Iaboratory,
Page 3 of 5
11 of21
37 of80
Calibmton Certflcab ID
NA1 548-038-030823-ACC-USL MEfnER TOTEDO $ervice
Test Equipment
All weights used for metrological testing are traceable to national or international standards. The weights were calibrated and certified by
an accredited calibration laboratory.
WephtSet 1: OIML E2
Weight Set No.:
Certiflcate Number:
Remarks
421 Oate of lssue:
Calibration Due Date:
07-Dec-2022
220635345-1 31-Dec-2023
Value of the built-in weight adjusted
Performed a linearity adjustment
End of Asedlbd Sedion
The information below and any attachments to this calibration certificate are not part of the accredited calibration.
Software VeBion: 1.23.1,70
Reporl VeEion: 2. 1 6.32
Fom Number AF1702Lrl.0
@ METTLER TOLEOO
This is an original document and may nol be partially reproduced without the
written permission of the issuing @libration laboratory,
Page 4 of 5
12 ol 21
38 of80
Calibration C€rtificab lD
NA1 548-038-030823-ACC-US L MEITLER TOIED0 Sorvice
Measurement Uncertainty of the Weighing lnstrument in Use
Stated is the expanded uncertainly with k=2 in use. The formula shall be used for the estimation of the uncertainty under consideration of
the errors of indication. The value R represents the net load indicalion in the unit of measure of the device.
Temperalure coefficienl for the evaluation of the measurement uncertainty in use:
Temperature range on site for the evaluation of the measurement uncertainty in use:
Linearizaton of Uncedalnv Equalion
2.o.io'6/K
4K
To optimize the stability of the linearization, besides of the zero load only increasing measurement points with a test load of 5olo of the
measurement range or larger are taken for the calculalion of the linear equation.
AbsolrJto and R6lativ6 Measur€ment Uncertainty in UBe brVadous N€t lndlcaflons (E)Gmpl€s)
i
1t.
I ',
II
II
g. .l
c 00c1 0.411
As L€rf,
{)r 1
RGrdtng lgl
001
Software Ve6ion: 1 .23.1.70
Report Ve6ion: 2. 1 6.32
Fom Number AF1702Lr1.O
@ METTLER TOLEDO
This is an original document and may not be partially reproduced without the
written permission of the is6uing €libration laboratory.
Page 5 of 5
13 of 21
39 of80
Attachment to Callbrauon Cortfi cab:
NA1 548-038-030823-ACC-U SL
Manufacturer Tolerance Assessment
MEffiER TOLEDO Service
Man ufactu rer Tolerance Assessment
Assessment done without considering measurement uncertainty.
The measurements from the attached calibration certificate were assessed against METTLER TOLEDO tolerances defined in SOP'Test and
Measurement Procedures for METTLER TOLEDO balances, Document: 10000018502.
Overall
As Left
{
{
{
{
{
As Found
{
{
{
{
N/A
Repeatability
Eccentricity
Linearity
Sensitivity
Measurement Results
Repeatability
Ted Load: 100 g
1 100.0003 g 100.0001 s
2 100.0002 g 100.0000 g
3 100.0002 g 100.0000 g
4 100.0002 g 100.0000 g
5 100.0001 g 100.0001 s
6 100.0002 g 100.0000 g
7 100.0002 g 99.9999 g
I 100.0000 g 100.000'l g
o 100.0003 g 100.0001 g
10 100.0002 g 100.0002 g
Shndard
Dwlauon 0.00009 g 0.0@08 g
TolsEnce 0.000109 {0.0@'l0g {
Software Version: 1 23.'1.70
Report Vecion:2.1 6.32
Fom Number AF'1702L/1.0
O METTLER TOLEDO
This is an original document and may nol be partially reprodu@d withoul the
written pemission of the issuing €libmtion laboratory.
Page 1 of 2
14 ot 21
40 of 80
Attaciment io Callbratlon C€r0ficab:
NA1 548-038-030823-ACC-USL
Manufacturer Tolerance Assessment
METTTER TOTEDO Service
Eccentricity
Test Load:50 g
Muimum
Do\riaton 0.(x)01 g 0.0000 g
Toloranco o.ooo3os {0.0@3Os I
. The maximum deviation is determined as the absolute value of the largest deviation from the center.
Linearity - Difiercntial Method
As Found
N/A 20.0000 g 20.0002 s 0.00006 s
J 2og 20.0000 g 20.0002 g 0.00012 g
4 4os 20.0000 s 20.0001 g 0.00008 g
5 6os 20.0000 g 20.0001 g 0.00004 g
6 80s 20.0000 g 20.0001 g 0.00000 g
8 NiA 100.0000 q 1 00.0003 q N/A
The As Found Sensitivity Tolerance is only valid if the device has been adjusted before the test.
As L€rft
-inoaritv Dsviation 0.000't2 g
-lnoarlty Toleranca 0.ooo2 s {
-lnoarltv DeYlatlon 0.00000 g
-in6arity Toloranc€0.0002s {
The values in column 'Deviation" and the "Linearity Deviation"
* This point was used to satisfy the sensitivity requirement.
iensitivity Deviation 0.0003 g
lonsltlvlty Toleranco N/A
Sensltlvlty Devlatlon 0.0001 s
len!ltlvltv To16ranco O.OO08 o n
are zero point offset and sensitivity error compensated.
N/A 20.0000 g 20.0000 g 0.00000 g
J 20s 20.0000 s 20.0000 g 0.00000 g
4 4og 20.0000 g 20.0000 g 0.00000 g
5 60g 20.0000 g 20.0000 g 0.00000 g
6 80s 20.0000 g 20.0000 g 0.00000 g
8',N/A 100.0000 g 100.0001 s N/A
Software Version: 1 23.1 .70
Repon Version: 2.1 6.32
Fom Numbef, AF1702111.0
O METTLER TOLEDO
This is an original document and may not be partially reproduced without the
writlen permission of the issuing elibration laboratory.
Page 2 oI 2
15 of 21
41 of80
Calibration Certificab lD
NAI 548-039-030823-ACC-USL
Mettler Toledo, LLC
'1900 Polaris Parkway
Columbus, OH43240
l.8OO.METTLER
Customer
ah
IIE-cnBTtEI
METTLER TOTEDO
Accredited by the American Association
for Laboratory Accreditation (A2LA)
CALIBRATION CERT #1788.01
ISO 17025 Accredited
ANSYNCSL 2540-1 Accredited
Accuracy Galibration Gertifi cate
Alliance Source Testing
5530 Marshall St
Gompany:
Address:
Clty:
Zip / Poshl:
State / Pmvincs:
Weighing Device
Arvada Contac-t:Eric Grosiean
80002-3108
Colorado
Manufac'turer:
Model:
Serial No.:
Building:
Floor:
Room:
Denver
TB-6201
lnstrument Type:
A$ot Numben
Teminal Model:
Teminal Serhl No.:
TeminalAsset No.:
Weighing lnstrument
N/A
1 79041 89 N/A
5520
Lab
1 6200 s 0.1 s
N/A
N/A
Procedure
Calibration Guideline:
METTLER TOLEDO Work lnstucffon:
ASTM E898.20
30260953 v1.61
This calibration certificate including procedures and uncertainty estimation also complies with EURAMET cA18 v 4.0.
This calibration certificate contains measurements for As Found and As Left calibrations.
The sensitivity/span of the weighing instrumenl was adjusted before As Left calibration with a buill-in weight.
ln accordance with EURAMET cg-l8 (1 1/2015), the test loads were selected to reflect the specific use of the weighing device or to
accommodate specific calibration conditions.
As Found Start: 20.8'C End: 20.5 "C Start: 20.0 % End:21.0 o/o
As Left Start:20.1 "C End:20.1 'C Start: 20.9 % End: 21.0 o/o
This certificate is issued in accordance with the conditions of accreditation granted by MLA, which is based on ISO/IEC 17025. MLA
has assessed the measurement capability of the laboratory and its traceability to recognized natlonal standards.
Environmenlal conditions have been
verified to ensure the accuracy of the
calibration.
As Found Callbratlcn DatB:
As l-eft Calibnation Date:
lssue Date:
R€queetod Noxt Calibration Date:
08-Mar-2023 Authoriz€d A2lA SignatoM
[ .-*" i-t.-
08-Mar-2023
08-Mar-2023 Chris Carson
31-Mar-2024
Softwaro VeBion: 1.23,1.70
Reporl VeEion: 2.16.32
Fom Numberi AF1702Lr1.0
@ METTLER TOLEDO
Thjs is an original document and may not be partially reproduced without the
written permission of the issuing @libralion laboratory.
Page 1 of4
16 of 21
42 of 80
Galibration Certificab lD
NA1 548-039-030823-ACC-USL METTTER TOTEDO Service
Measurement Results
Repeatability
Test Load:2000 g
O As Found
I As Left I {T0st Poinl)
>6d
. 4d.
3d,
-.26.
,ld
o
Standad 0.009 I 0.009Dgt/iation
Eccentricity
4
The "d" in the graph represents the readability of the range/interual in which the
test was performed.
The results of this graph are based upon the absolute values of the differences
from the mean value.
(o)
o
(o
(.1
o)
Tost Load:2000 g
Maxlmum 0.1 s I 0.1 gDevlaton
Error of lndication
The "d" in the graph represents the readability ofthe range/interval in which
the test was performed.
As Found As Left
As Found
1 o.o g o.o g o.o g 0.06 g 2
2 1000.0 g 999.9 g -0.1 g 0.09 g 2
J 3000.0 g 2999.9 g -0.1 s O.12 s 2
4 4000.0 g 3999.8 g -o-29 0.14 g 2
R 6000.0 g 5999.8 g -0.2 g 0.19 g 2
43 of 80
Software VeBion: 1.23.1.70
Report VeEion: 2.1 6.32
Form Number: AF1702Lr1.0
O I\,1ETTLER TOLEDO
This is an original document and may not be partially reproduced without the
writlen permission of the issuing calibralion laboratory.
Page 2 of 4
17 of 21
Calibration Cerlificab lD
NAI 548-039-030823-ACC-USL METTTER TOTEDO Service
tu Left
o.o s o.o g o.o g 0.06 g 2
2 '1000.0 g 1000.0 g o.o s 0.09 g 2
J 3000.0 g 3000.0 g o.o s 0.12 g 2
4 4000.0 s 4000.0 s o.o g 0.14 g 2
5 6000.0 g 6000.1 g 0.1 s 0.19 g
<} AstEfr
For improved legibility of the graphics
only increasing measurement points
are shown and measurement points
close to zero are not displayed.
"
--._
';;,t- ,{{}oo .otro .1(r{r(l
Callbratlon Poinlr lgl
The uncertainty stated is the expanded uncertainty at calibration obtained by multiplying the standard combined uncertainty by the
coverage factor k - which can be larger than 2 according to ASTM E898 and EURAMET cg-18. The value of the measurand lies within the
assigned range of values with a probability of approximately 95%.
The user is responsible for malntaining environmental conditions and the settings of the weighing instrument when it was calibrated.
Test Equipment
All weights used for metrological testing are traceable to national or international standards. The weights were calibrated and certified by
an accredited calibration Iaboratory.
.g
I
G
.9Ec:o
BbL!
O As Found
0 .1*---..
0;t i
c +".*"
WoightSet 1: OIML Fl
Weight Set No.:
Certificate Number:
Remarks
685 Date of lssue:
Calibration Due Date:
12-Jan-2023
220642893-1 31-Jan-2025
N/A
End of Accr€dibd Secdion
The information below and any attachments to this calibration certiflcate are not part of the accredited calibration.
Software Ve6ion: 1.23.'1,70
Report Vereion: 2.1 6,32
Fom Number; AF1702Lrl.0
O METTLER TOLEOO
This is an original document and may not be partially reproduced withoul the
writlen permission of the issuing €libration laboratory.
Page 3 of 4
18 of 21
44 of80
Calibraton Cerdflcah lD
NA1 548-039-030823-ACC-USL METTTER TOTEDO Service
Measurcment Uncertainty of the Weighing lnstrument in Use
Stated is the expanded uncertainty with k=2 in use. The formula shall be used for the estimation of the uncertainty under consideration of
the errors of indication. The value R represents the net load indication in the unit of measure of the device.
Temperature coefficient for the evaluation of the measurement uncertainty in use:
Temperature range on site for the evaluation of the measurement uncertainty in use:
Lineariza$on of Uncerbln$ Equation
6.0 . 10'6 / K
To optimize the stability of the linearization, besides of the zero load only increasing measurement points with a test load of 5% of the
measurement range or larger are taken for the calculation of the linear equation.
Absolub and Relaliw Measumment Uncertalnty in Uee forVarlou8 Net lndicatons (E(amples)
l{)(l
,(\
r (.'
.,:il
6K
Ti
T
ItI
t
8.,
b!oI
i
e'j
Software Ve6ion: 1.23.1.70
Report VeEion: 2.1 6.32
Fom Number: AF1702111.0
@ METTLER TOLEDO
This is an original document and may not be partially reproduced withoul the
writlan permission of the issuing €libration laboratory.
Page 4 of 4
19 of 21
45 of80
Athchmont b Callbratlon Certflcat€r
NA1 548-039-030823-ACC-USL
Custom Tolerance Assessment
MEITHR TOLEDO Service
Custom Tolerance Assessment
Assessment done without considering measurement uncertainty.
One or more of the measurements from the attached calibration certificate were assessed against customer-defined tolerances.
Overall
As Le
{
{
{
{Error of lndication
Repeatability
Eccentricity
As Found
{
{
{
{
Measurement Results
Repeatability
T€st Load:2000 g
SlandaId
Devldon 0.00 s 0.00 g
Tol€lanoa 0.109 ./0.109 ./
Eccentricity
Test Load:2000 g
Ma)dmum
Dsrldon 0,1 c 0.1 s
Tol6lance o.3s {o.3s {
Softwaro Version: 1 23.1.70
Report Version: 2,'1 6.32
Fom Number AF1702111.0
O METTLER TOLEOO
This is an original document and may not be partially reproduced without the
written permission of th6 lssuing @libration laboratory.
46 of 80
20 ot 21
Page 1 of2
Attadrnent b Callbratlon CerEncate:
NAI 548-039-030823-ACC-U SL
Custom Tolerance Assessment
MEITTER TOTEDO Service
Eror of lndication
As Found
As Left
Software VeEion: 1 23.'1.70
Report Version: 2.16,32
Fom Number AF1702Lr1.0
O METTLER TOLEDO
This is an original document and may not be partially reproduced without the
written pormission of the issuing Blibration laboratory.
Page 2 of 2
21 o121
47 of80
,At\ptllfl"h-
PARTICLE SIZE DATA SUMMARY
SAMPLE ID
CUMUIANVE NUMBER % LESS THAN INDICATED
SIZE(uml
NUMBER
WEIGHTED
MEAN
{rrml10h Percentle 50s Percentlle 90h Percentlle
M5 Rinse Residue
M5l2O2 - SME005 - Run 'l Cont. 2 - 32460 0.53 0.68 1.46 1.08
M51202 - SME005 - Run 2 Cont. 2 - 32468 0.54 0.72 1.73 1.17
MSl202- SME005 - Run 3 Cont. 2 - 32469 0.53 0.67 1.53 1.12
M5 Acetone Blank - 32458 0.53 0.64 1.05 0,84
SAMPLE ID
CUMULATIVE VOLUME % LESS THAN INDICATED
SIZE (um)
VOLUME
WEIGHTED
MEAN
luml10h Percentile 50th Percentile 90s Percentile
M5 Rinse Residue
M51202- SME005 - Run 1 Cont. 2 - 32460 8.93 23.25 144.02 42.58
M51202- SME005 - Run 2 Cont. 2 - 32468 8.55 46.15 197.62 92.59
MSl202- SME005 - Run 3 Cont. 2 - 32469 8.51 21.17 67.51 34.72
M5 Acetone Blank - 32458 12.26 36.20 91.92 42.99
PARTICLE SIZE DATA SUMMARY
SAMPLE ID
CUMULAIVE VOLUME % LESS THAN OIAMETER (um)
2.5 pm 10 pm
Quartz Filter
M5l2O2- SME005 - Run 1 Cont. 2 - 32460 1.2 12.9
MS|2O2 - SME005- Run 2 Cont. 2-32468 1.2 13.5
MS2O2- SME005 - Run 3 Cont. 2 - 32469 1.2 14.2
M5 Acetone Blank - 32458 't.6 6.9
PRelruuxARY REsuLTs PTL Proiect #6{577-62
N?&)-t2-t3
tlt t tr 11.rl48 of 80
,.#\ptl Particle Technology Labs
555 Rogers Street, Downers Grove. lL 60515
630.969.2703
www.partlcletechlabs.com
INTERPRETING YOUR SINGLE PARTICLE OPTICAL SENSING ANALYSIS
lntroductlon
Your samples have been analyzed on a Particle Sizing Systems AccuSizer770, 780, or A7000 System, a particle counter capable of determining
both particle size and concentration of suspensions. The AccuSizer utilizes Single Particle Optical Sensing (SPOS) lechnology (also referred to
as the photozone technique) to provide excellent resolulion, wide dynamic range, and high accuracy.
SPOS utilizes two physical principles of detection; light extinction (also known as light obscuration) for particles larger than approximately '1.5 Um
and light scattering for particles smaller than 1.5 pm. During analysis, a dilute suspension of particles is passed through a region of uniform
illumination produced by a laser diode. Parlicles greater than approximalely 1.5 Um are detected by the amount of light they obscure to the
extinction detector, while smaller particles are detected by the intensity of light scattered at a range of angles towards a separate detector. The
particle size is then determined by comparing the pulse heights to a calibration curve generated with standard reference materials of known size.
The data are presented on the basis of CIRCULAR EOUIVALENT DIAMETEH. This analytical technique is summarized under ISO 21501-2,2007
Determination of pafticle size distribution -- Single pafticle light interaction methds - Part 2: Light scattering liquid-bome particle counter and ISO
21501-3:2007 Determination ol parlicle size distribution - Single particle light interaction methods - Part 3: Light extinction liquid-borne pafticle
counter.
All AccuSizer systems consist of a pulse height analyzer, fluidics module, and sensor.
Pulse Height Analyzer Commonly refened to as the "counter box," the pulse height analyzer converts pulses from the sensor into particle size.
AccuSizer pulse height analyzers are multichannel and can report results in up to 1024 size channels, providing excellent
resolution.
Fluidics Module The fluidics module determines how sample is transported through the sensor. Multiple fluidics configurations are
available at PTL: including auto-dilution, metered drain, and syringe injection. The most appropriate for your sample was
selected depending on the parlicle concentration and other sample characteristics.
Sensor Panicles flowing through the sensor scatter and obscure laser light, creating pulses proportional to the parlicle size.
Particles must pass the sensing zone one at a time to prevent what are known as coincidence errors. Hence, dilution in
a clean, chemically compatible tluid is often required. While multiple sensor models are available for the AccuSizer, lhe
most commonly used model at PTL is the LE400 sensor with a nominal range of 0.5 pm to 400 pm.
Since SPOS analyzers are true particle COUNTERS, data can be reported in two formats - NUMBER (count or frequency) and VOLUME. For
your reference, the data have been reported using both of these formats. The 10h, 50h, and 90th percentiles on both the NUMBEB and VOLUME
6asis are also summarized. These percentiles will indicate the particle size where the percentage of the distribution lies below. For example, a 90h
percentile value of 10 pm indicates that 90% of the distribution lies below 10 gm.
Number (Count or Fruquency) Data
Your data will include a NUMBER WEIGHTED DIFFERENTIAL FREQUENCY histogram, which plots the percentage of paflicles detected versus
the size of the particles detected, on a log scale. The particle size distribution (PSD) is constructed particle by particle meaning each particle
has equal weighting. For instance, a 1 pm particle will have just as much impact on the distribution as a 100 pm particle. The number data
are the primary ouput of the AccuSizer and are used to generate all other outputs.
Since the instrument counts individual particles and a known volume ol sample is analyzed, an accurate concentralion value in units of particles/ml
can be generated.
Volume Data
Your data will also include a DIFFERENTIAL VOLUME PERCENTAGE graph, which plots the volume-weighted percentage of particles detected
yersus the size of the particles detected, on a log scale. The volume data are generated by assuming each particle is spherical, converting the
diameter into a spherical volume to give each particle a weighting relative to its volume. Since the volume ol a parlicle increases proportionally
to the diameter cubed (D3), the volume data are inherently weighted towards the larger particles and better represent where the bulk or mass
ol the system lies. For example, a spherical 1 !m particle will have a volume of 0.52 pm3 while a 100 pm spherical particle will have a volume of
approximately 523,599 pm3. One would have to count roughly one million, 1 pm particles in order to contribute the same volume percentage as
one, 100 pm particle. The volume distribution can be considered interchangeable with a mass distribution if all the particles can be assumed to
have equivalent density.
Channel Data
Channel data are also provided, which present the data within each channel or bin in a tabular format. The diameter in micrometers, the number
of particles detected of thal size, the cumulalive number of particles, number and volume percentages, and absolute volume values can be found
in this section.
For additional questions specific to your analysis resu/ls, please contact us directly.
49 of 80
llis report mnfans to prolbitxs d 21 CRpart 11
,dN Particle Technology La bs
tbff Becly FErifrqt
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Slc,vrEss:10.8 gn
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50 of80
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This reportconfonm to povbi:rs d 21 CRpart 11 ifrlm.- SN,E05- tun I Gnt. 2-P4&- pctnnrepori- 1211?l2W 13:52:48- hgcl of 4
lN Particle Technotogy Labs
Qerdor: Becky l-hniltct
Ha cobctim dddtnD:'1351 IZPAW
'i0cl
HdTine: 13i,52 121 12I2W
TargetcmcenHixl: 70m
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10 0.532 Ln6 8.925
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Chrnnel Diantrter
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Coruts
(#)
Cuuladrr
(#SDl&)
Nur&r
ea
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(%SDia.)
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(%sIXa.)
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57 0.526 4//.20 44420 7.4 0.5 0.0 74 0.0 3383.0
58 0.54 436f'5 88@5 t-)0.5 0.0 14.7 0.0 3680.4
59 0.563 3r743 lln69 5.3 0.4 0.0 20.0 0.0 2971.7
60 0.584 41632 161401 7.0 0.6 0.0 27.0 0.4335.7
6l 0.606 3%21 200821 6.6 0.6 0.0 33.6 0.4597.0
62 0.629 37030 237852 6.2 0.6 0.0 39.8 0.4834.2
63 0.655 40053 27790/.6.7 0.7 0.0 46.5 0.5890.5
g 0.682 29786 306@0 4.8 0.6 0.0 5 1.3 0.1 4795.7
55 0.712 31949 338639 5.3 0.7 0.0 56.7 0.2 &29.6
$0.74 n$3 36rU2 3.8 0.5 0.0 @.4 0.2 4835.6
67 0.779 243t6 385388 4.1 0.6 0.0 64.5 0.3 fln9.1
68 0.815 20s96 405984 3.4 0.6 0.0 67.9 0.3 5830.9
69 0.852 E05l 42435 3.0 0.5 0.0 10.9 0.3 s851.8
70 0.8v2 &39 4D74 3.1 0_6 0.0 74.0 0.3 6770.9
71 0.932 2r76 454650 2.1 03 0.0 16.1 03 5247.9
T2 0.912 2U6 457496 2.1 0.5 0.0 18.2 0.4 6192.5
73 .0ll %t3 4'76910 ,6 0.4 0.0 79.8 0.4 5100.7
74 .051 9437 486v7 ,6 0.4 0.0 81.4 0.5 5729.7
75 .0e0 8393 49t7N ,4 03 0.0 82.8 0.5 sM.4
76 130 8r 19 5m859 4 0.4 0.0 u.l 0.5 6135.7
77 170 ffi 508899 .0 0.3 0.0 85.1 0.5 5U0.7
18 .2tl 62v)5 l5 l9l 0.4 0.0 86.2 0.6 5857.6
79 .253 5070 524261 0.8 0.3 0.0 87.0 0.6 5m.9
80 .29s 4@ 52472t 0.7 0.3 0.0 87.8 0.6 5074.9
81 .338 4W 528820 0.7 0.3 0.0 88.s 0.6 51!/..3
n .382 4f,65 532885 0.7 03 0.0 89.2 0.7 5619.2
83 .4n 3c97 535983 0.5 0.3 0.0 8.7 0.7 47fi.6
&l 473 3170 539153 0.5 0.3 0.0 90.2 0.7 5306.5
85 .521 3314 y2M 0.6 03 0.0 90.8 0.8 6r0zl
86 .570 25n 545058 0.4 0.3 0.0 91.2 0.8 5250,6
s7 .621 n37 fl7796 0.5 0.3 0.0 9t_7 0.8 6104.5
88 .674 u54 s50250 0.4 03 0.0 y).1 0.8 6029.0
89 7n N)9 552279 0.3 02 0.0 92.4 0.9 5499.0
90 788 2120 55439 0.4 0.3 0.0 v2.8 0.9 6350.7
52 of 80
thb reportconfonstoprovbiors of 21 CFRpart 11 l{6A92- SI!E)05- Rm 1 Ont. 2-324il- pct runreport- 1U1?J2gn13:52:.48-P4ezd 4
Channel Di.ttrter
(run)
Cannts
(f)
Cmrulatire
65Dir.)
Number
(w
Arcrgt Volunr(n Nuder
f/oSDia.)
Volum
(%SDig.)
Ah.Volunn
A"rfl
9l 1.850 t729 5561n 0.3 0.2 0.0 93.t 0.9 5733.9
92 1.916 1880 558007 0.3 0.3 0.0 93.4 .0 6924.7
93 1.986 ta1 559654 0.3 0.3 0.0 %.6 .0 6757.7
94 2.061 1676 561330 0.3 0-3 0.0 93.9 .0 76U.6
95 2.139 598 5Ov28 0.3 0.3 0.0 %.2 I 8188.8
95 2.220 348 56/,276 0.2 0.3 0.0 %.4 .l n21.6
97 2.3U 384 555660 0.2 0.3 0.0 %.6 .2 88s9.s
98 2.391 270 s66930 0.2 0.3 0.0 %.9 2 9089.8
I 2.4n 143 568073 0.2 0.3 0.0 95.0 .2 9147.5
r00 2.576 184 569257 0.2 0.3 0.1 9s.2 .3 10595.5
l0l 2.673 1089 570345 0.2 0.3 0 95.4 A r0894.7
t07 7,775 ta52 571398 0.2 0.3 0.1 95.6 4 763.5
103 2.880 1067 572464 0.2 0.4 0.1 95.E .5 3342.2
t04 2.W 1050 573514 02 0.4 0.1 96.0 .6 4689.0
t05 3.103 947 574462 0.2 0.4 0.1 96.1 .6 4823.8
r06 3.221 960 57v122 0.2 0.4 0.1 96.3 7 6810.8
107 3.y4 953 576375 0.2 0.4 0.1 96.4 ,8 8660.3
l0E 3.472 835 577210 0.1 0.4 0.1 96.6 ,9 8301.4
109 3.&897 578107 0.2 0.5 0.1 96.7 2.0 1989.5
0 3.74 668 578775 0.1 0.4 0.1 96.8 2.r 8317.2
I 3.8E5 8s6 579631 0.1 0.5 0.1 n.0 2.2 2OU.4
4.034 668 580298 0.1 0.4 0.1 n.l 2.3 22949.0
l3 4. tE9 690 580988 0.1 0.5 0.1 97.2 2.5 26553.6
l4 4.350 ffi 581654 0.1 0.5 0.1 97.3 2.6 28683.s
l5 4.5t7 634 s82288 0.1 0.5 0.2 n.4 2.8 30588.8
l6 4.691 757 583045 0.1 o.7 0.2 n.6 3.0 ,10908.6
17 4.871 &6 583651 0.1 0.6 0.2 n.7 3.1 36679.0
l8 5.059 660 58431 r 0.1 0.7 0.2 97.8 3.4 44757.9
t9 5.2s6 619 584930 0.t 0.7 0.2 97.9 3.6 47057.9
20 5.452 6t2 5855r'.2 0.t 0.8 0.3 98.0 3.9 9t'72.9
I 5.677 5n 586139 0.0.8 0.3 98.1 4.1 57167.4
22 5.%2 586 586n4 0.t 0.8 0.3 98.2 4.5 63@.1.7
23 6.138 4l 587185 0.1 0.7 0.3 98.2 4.7 55751.3
24 6.383 563 587748 0.0.9 0.4 98.3 5.1 76r,88.7
,<6.639 st2 588249 0.0.9 0.4 98.4 5.5 76U6.5
26 69U 528 585n7 0 .0 0.5 98.s 6.0 90934.5
27 7.t79 503 589281 0.I 0.5 98.6 6.4 v745.0
128 7.4&4J6 5897r9 0..0 0.5 98.7 5.9 95r'0,6.4
29 7.758 459 s90178 0 I 0.6 98.7 7.5 tr2143.9
30 8.051 ffi 590618 0.0.6 98.8 8.1 no68f.2
3l 8.372 zl08 59W26 0 2 0.6 98.9 8.7 t2955.2
32 8.590 436 591462 0..4 0.7 99.0 9.4 t4994/..5
)J 9.0r6 4t4 591n6 0..4 0.8 99.0 10.2 158839.2
34 9.347 44 592320 0..5 0.9 99.t 2 tw737.9
35 9.682 375 sm@s 0..4 0.9 99.2 2.0 178108.2
36 10.020 343 593038 0.0.9 9.2 ,o 180750.3
31 r0.365 296 s93335 0.0 .3 0.9 9.3 3.8 1728,9.2
38 10.720 274 5936f9 0.0 J 0.9 9.3 147 t76798.9
39 I 1.084 2n s93896 0.0 .5 1.0 99.4 t5.7 2C/.753.0
140 l 1.458 295 594191 0.0 6 1.2 99.4 r6.8 23205/'.5
l4l I l.&il 213 s9443 0.0 .2 0.9 9.5 17.8 tu7'79.4
142 12.232 2tl s94614 0.0 .3 .0 99.5 18.8 20r92s.s
143 t2.631 n9 594843 0.0 ,5 2 9.5 20.0 2420rc.9
t4 13.036 203 595046 0.0 ,4 2 9.6 21.1 235790.6
145 t3.4"1 222 59s268 0.0 1.6 4 9.6 n.5 24y3.5
t46 t3.863 1A 59y31 0.0 1.3 9.6 23.7 22630t.1
147 14.281 l8t 59561 I 0.0 1.5 4 9.7 25.0 275837.6
148 4.7(n l5l 5957(t3 0.0 1.3 .2 9.7 26.3 251 198.8
149 l5 n7 r5l 595914 0.0 t.4 .c 9.7 n.6 273212.3
150 15.531 159 596072 0.0 t.6 .5 9.7 aoa 310937.0
151 15.943 t44 s96216 0.0 1.5 1.5 99.8 30.7 304656.6
53 of 80
This reportconfonsto provbirs of 21 CFRpart 11 11612}2- SlVEmS- Rln 1 &nt. 2-32ffi- pct rurn rryl- 121224813:52:.48- hge3 of 4
Channel Diamter
[tnt)
Counts
(#)
Cumulatiw
$SDia.)
Number
(w
Arta
ea
Volum
ea
Nunter
(%SDia)
Vdunn
(%SDia)
Abe, Volutt*
(rrnf)
152 16.353 ll6 59633 I 0.0 1.3 3 99.8 32.0 2&7n.1
153 16.163 l0l s9&32 0.0 t.2 .2 99.8 33.2 2483@.4
154 17.176 121 596553 0.0 1.5 .6 99.8 34.8 321 61 1. I
155 17.595 86 s96639 0.0 l.l .2 9.8 36.r 2M5t.3
56 18.u22 103 596742 0.0 t.4 .6 99.8 37.6 3143s6.0
5'7 t8.462 6'l s96809 0.0 0.9 I 9.9 38.1 n196.4
58 18.919 67 596n6 0.0 1.0 .2 99.9 39.9 23W37.3
59 19.39 65 59694t 0.0 1.0 .2 9.9 4t.l 24%n.4
160 19.908 62 59003 0.0 1.0 .3 9.9 42.4 29227.1
l6l 20.47 58 597ofi 0.0 1.0 J 9.9 43.7 2587fi.0
t62 2l 015 4t 597 r0r 0.0 0.7 .0 99.9 4.7 199352.8
r63 21.608 60 59716t 0.0 .6 99.9 4.2 3 r5203.0
t64 22.n4 48 597210 0.0 1.0 .4 9.9 47.6 nq$t.3
l6s 22.80 50 597260 0.0 l.I .6 9.9 49.2 3149r6.2
r66 23.512 4l 597301 0.0 0.9 .4 99.9 50.6 nnt2.1
t67 24.177 )z 5n$3 0.0 0.8 .2 9.9 51.7 234s79.1
68 24.U9 12 5n355 0.0 0.6 0.9 99.9 s2.6 179182.8
69 25.94 25 597381 0.0 0.7 I 100.0 53.8 22'7257.3
70 26.24 22 597/04.0.0 0.6 .0 100.0 54.8 210767.4
26.890 1's97435 0.0 0.9 .6 100.0 56.4 3U4.9
72 27.59t 591456 0.0 0.6 100.0 57,5 225575.9
73 28.303 597474 0.0 0.6 100.0 58.6 221374.4
74 29.030 5n486 0.0 0.4 0.7 100.0 s9.3 143315.2
75 29.77t 597502 0.0 0.6 1.2 t00.0 60.s 231861.6
76 30.528 5975t9 0.0 0.6 t.2 100.0 6t.7 2500t7.2
77 31.304 2l 597fi 0.0 0.8 r.6 100.0 63.4 329450.0
78 32.W l5 s97555 0.0 0.6 1.3 r00.0 &.6 2583?5.7
79 32.916 9 5qs64 0.0 0.4 0.9 100.0 65.5 n4143
80 33.758 l5 597579 0.0 0.7 1.5 t00.0 67.0 300486.0
8l 34.627 7 597586 0.0 0.4 0.8 r00.0 67.8 t62tst.2
s2 35.527 6 597s92 0.0 0.3 0.7 r00.0 68.5 t31347.6
83 36.462 7 597599 0.0 0.4 0.9 100.0 @.4 189324.2
184 37.436 l3 5916t2 0.0 0.8 1.8 100.0 7t.2 3s8583.0
185 38.4y 4 597616 0.0 0.2 0.6 100.0 71.1 I I 1040.2
r86 39.s20 4 5n620 0.0 0.2 0.5 100.0 7)7 120529.2
187 40.628 4 597624 0.0 0.3 0.7 100.0 73.0 r30951.9
188 4t.772 597631 0.0 0.5 t.4 tm.0 74.4 2U&.0
189 4.954 4 597635 0.0 0.3 0.8 100.0 75.2 154756.8
190 4.174 0 597635 0.0 0.0 0.0 r00.0 75.2 0.0
t9l 45.434 0 5n$5 0.0 0.0 0.0 100.0 75.2 0.0
tE2 46_736 4 597638 0.0 0.3 1.0 100,0 76.1 199340.8
193 48.080 5 5na4 0.0 0.5 t.6 100.0 77.8 3?5552.8
194 49.44 4 s97&8 0.0 0t t.2 100.0 78.9 236373.3
195 50.900 2 597650 0.0 0.2 0.6 t00.0 79.6 128757.0
196 s2.380 2 597652 0.0 0.2 0.7 100.0 80.3 1403 I 5.7
t91 53.907 2 597653 0.0 0.2 0.8 r00.0 8r.0 152955.0
198 55.485 4 597657 0.0 0.5 1.7 100.0 n.7 333557. I
t99 51.t14 0 597657 0.0 0.0 0.0 100.0 82.7 0.0
200 58.795 4 59766t 0.0 0.5 2.0 100.0 u.7 396890.0
201 60.s31 0 59766t 0.0 0.0 0.0 100.0 u.7 0.0
2A 62323 0 597661 0.0 0.0 0.0 100.0 u.7 0.0
203 &.1"t3 0 s976r,1 0.0 0.0 0.0 100.0 u.7 0.0
2M 55.082 0 597661 0.0 0.0 0.0 100.0 u.7 0.0
205 68.0s2 0 5n6t 0.0 0.0 0.0 100.0 u.1 0.0
206 70.086 0 s97661 0.0 0.0 0.0 100.0 u.7 0.0
207 72.|U 0 s97661 0.0 0.0 0.0 100.0 u.7 0.0
208 74.349 0 597661 0.0 0.0 0.0 100.0 u.7 0.0
2@ 76-Sn 0 s976t 0.0 0.0 0.0 100.0 u.7 0.0
210 78.885 0 597651 0.0 0.0 0.0 t00.0 u.7 0.0
2l 81.260 0 597661 0.0 0.0 0.0 lm.0 u.7 0.0
'r1)83.709 0 59766t 0.0 0.0 0.0 t00.0 4.7 0.0
54 of 80
This reportconfonstoprovisions of 21 CFRpart 11 l\frfNZ- StvE0Os- fun 1 Gnt.2-n4ffi- pctrunreport- 1211212sn13.52:.48- hge4of 4
Channel Dianeter
Gnt)
C.drnts
(#)
CurmdctitD
(#SDi&)
Number
(w
Alte
(vd
Volunn
vd
Nunfter
(%sDia.)
Volune
(%SDir.)
Ah"Volum
(um3)
2t3 86.233 0 svt6t 0.0 0.0 0.0 100.0 u.7 0.0
214 88.834 0 59766t 0.0 0.0 0.0 100.0 u.7 0.0
2t5 91.515 0 597(trl 0.0 0.0 0.0 100.0 u;1 0.0
2t6 9t1.276 0 597661 0.0 0.0 0.0 100.0 u;7 0.0
2r7 97.1 l8 0 597661 0.0 0.0 0.0 100.0 u.7 0.0
218 100.044 0 597661 0.0 0.0 0.0 100.0 u.7 0.0
219 103.052 0 597661 0.0 0.0 0.0 100.0 84.7 0.0
220 106.143 0 597661 0.0 0.0 0.0 100.0 u.7 0.0
22t t@3n 0 5976tr1 0.0 0.0 0.0 r00.0 u.7 0.0
222 t2.592 0 597661 0.0 0.0 0.0 100.0 u.1 0.0
223 5.956 0 597651 0.0 0.0 0.0 100.0 u.7 0.0
n4 19.418 0 5n6l 0.0 0.0 0.0 100.0 u.7 0.0
25 ?2.982 0 5n6t 0.0 0.0 0.0 100.0 u.7 0.0
?26 76.654 0 597661 0.0 0-0 0.0 100.0 u.1 0.0
27 30.438 0 597661 0.0 0_0 0.0 100.0 u.7 0.0
n8 34.341 0 s97ffi1 0.0 0.0 0.0 r00.0 u.7 0.0
229 138.366 0 s976r1 0.0 0.0 0.0 lm.0 gt.1 0.0
230 r42.5n 0 597ffil 0.0 0.0 0.0 100.0 u.7 0.0
231 146.815 2 5n6r,3 0.0 1.7 t5.3 lm.0 100.0 3089812.0
232 t5t.2s4 0 s976r,3 0.0 0.0 0.0 100.0 lm.0 0.0
233 155.845 0 5976r,3 0.0 0.0 0.0 100.0 100.0 0.0
234 160.600 0 597663 0.0 0.0 0.0 100.0 r00.0 0.0
235 t6s.527 0 5976f.3 0.0 0.0 0.0 100.0 100.0 0.0
?36 170.638 0 5976f,3 0.0 0.0 0.0 100.0 lm.0 0.0
237 t75.945 0 597663 0.0 0.0 0.0 100.0 r00.0 0.0
238 18t.tl6l 0 597663 0.0 0.0 0.0 100.0 100.0 0.0
239 r&7.201 0 5n6r,3 0.0 0.0 0.0 100.0 100.0 0.0
24 193. t8r 0 5976r,3 0.0 0.0 0.0 100.0 100.0 0.0
ul tw.v6 0 59766,3 0.0 0.0 0.0 t00.0 r00.0 0.0
242 20s.022 0 5976r,3 0.0 0.0 0.0 r00.0 100.0 0.0
243 249.O8 0 5n663 0.0 0.0 0.0 100.0 100.0 0.0
24 213.329 0 s9156,3 0.0 0.0 0.0 100.0 rm.0 0.0
245 216.67 0 597663 0.0 0.0 0.0 100.0 tm.0 0.0
246 DO.t9 0 597663 0.0 0.0 0.0 100.0 100.0 0.0
241 224.614 0 5976r,3 0.0 0.0 0.0 100.0 100.0 0.0
248 230.730 0 597&3 0.0 0.0 0.0 100.0 lm.0 0.0
249 239.503 0 5n6tr,3 0.0 0.0 0.0 100.0 100.0 0.0
250 2s2.0s0 0 5n6r,3 0.0 0.0 0.0 100.0 100.0 0.0
251 269.670 0 5n663 0.0 0.0 0.0 100.0 lm.0 0.0
252 294.551 0 597663 0.0 0.0 0.0 100.0 r00.0 0.0
253 329.270 0 5n6tr,3 0.0 0.0 0.0 100.0 lm.0 0.0
254 373.305 0 597663 0.0 0.0 0.0 100.0 100.0 0.0
255 423.030 0 597663 0.0 0.0 0.0 100.0 100.0 0.0
256 474.M n 5n6f,3 0.0 0.0 0.0 100.0 100.0 0.0
55 of 80
It*s ropat confans to povisinr of 21 CFRpart 11
A\ Particle Technology Labs
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[&an: 1.167 Fn
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'ltis reportcsrfsrrs to pro/bbrs of 21 CRpart 11 l\4y2@- $vE)05- tun 2 &nt. 2-U@- pGt rln rwort- 1?J12lM 14:00:40 - hB 1 cf 4
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h0ort Bteflins 14:fi 121 1?lNB
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Owts n6uedZrS$6rdaoilr*Fo.spri,qry-q,_ ffiJffi;ffilv
Totd cornts/rL (> 0.5 gr|: 46699/nL
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t0 0.536 l.l23 &551
t0 0.715 8.891 46.153
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Ctrnnel Dirnnter
0m)
Com6
(CI
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6SDta)
Nm$er(n Arer
(%)
VoIum(o Nurnber
(%SDie.)
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C/oSDh.)
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tu#)
57 0.526 44590 445n 6.4 0.4 0.0 6.4 0.0 3395.9
58 0.94 4//.35 89025 6.4 0.4 0.0 t2.7 0.0 3750.4
59 0.s53 322fi 12r315 4.6 0.4 0.0 t7.4 0.0 w22.8
6fr 0.584 422.61 163516 6.0 0.5 0.0 2i.4 0.0 Mt.t
61 0.606 39742 2$n7 5.7 0.5 0.0 a.l 0.4519.7
O 0.629 374r0 24[f87 i.4 0.5 0.0 y.4 0.4883.7
63 0.655 41698 2&,38s 6.0 0.6 0.0 40.4 0.6132.4
&o.6n 303n 3lnn 4.3 0.5 0.0 44;t 0.5041.9
55 0-7t2 3/,/,92 v't203 4.9 0.6 0.0 49.7 0.6509.6
6 0.744 21489 3ngz 3.6 n5 0.0 53.3 0.2 y94.3
67 0.779 2m7 400699 4.0 0.6 0.0 31.3 0.2 6v2t.t
68 0.815 24s/'3 425242 3.5 0.6 0.0 60.8 0.2 6948.5
o 0.852 Dffi1 47250 3.1 0.5 0.0 il.0 0.2 'nv.5
70 0.892 22274 469524 3.2 0.6 0.0 67.2 0.3 8268.8
7l 0.932 t56f/.485187 2.2 0.5 0.0 69.4 0.3 ffi4t.9
72 0.972 t6/.78 501665 2.4 0.5 0.0 71.8 0.3 7930.4
73 1.011 t2132 513797 7 0.4 0.0 73.5 0.3 6574.1
74 1.051 12851 52ffi8 .8 0.5 0.0 75.4 0.4 7fi2.1
75 r.090 r 1788 s1u36 7 0.5 0.0 n.0 0_4 79q7.6
76 1.130 t22\550659 7 0.5 0.0 78.8 0.4 9236.8
n 1.170 8963 559622 .3 0.4 0.0 80.1 0.4 7524.6
78 I.2n 9503 s69t25 .4 0.5 0.0 81.4 0.5 8847.6
79 t.253 8186 5n3lL .2 0.4 0.0 82.6 0.5 u32.7
80 t.295 7369 584681 1 0.4 0.0 83.7 0.5 83&r.s
8I r.338 6208 5m889 0.9 0.4 0.0 84.5 0.6 7791.8
g2 1.382 688?sw16 1.0 03 0.0 85.s 0.6 9519.6
83 .427 5245 603mt 0.8 03 0.0 86.3 0.6 7q79.4
84 .473 5 193 608214 0.1 03 0.0 87.0 0.6 86y2.5
85 .521 5245 61v59 0.8 0.4 0.0 87.8 0.7 9659.7
86 .570 4228 6t7687 0.6 0.4 0.0 88.4 0.7 8s63.8
87 .621 42fi 62rw?0.6 0.4 0.0 89.0 0.7 9365.8
88 .674 3830 625717 0.5 0.4 0.0 89.5 0.8 9410.7
89 730 326s 628W)0.5 0.3 0.0 90.0 0.8 8U9.4
90 788 335s 632338 0.5 0.4 0.0 00.5 0.8 r00s0.5
58 of 80
thb report conforns to prwisims of 21 CFRpart 11 l{612A2- Sl\,E)05- Rrn 2 OnL 2- 32468- p6t run report - 12J1?l2UnM:ffi:$ - ft0ezd 4
Channel Dianrter
Gm)
Comts
(CI
Cumulatiw
(#SDia)
Number
v0
Aiea
e/d
Vdum
{vd
Number
{o/o3l}ta.l
Volum
(%SDia)
Ab.Vdum
(urft
9l 1.850 nw $5044 0.4 0.3 0.0 90.9 0.9 8979.0
92 1.916 2732 $m'l 0.4 0.3 0.0 91.3 0.9 l{n65.0
93 1.986 2423 ffi199 0.3 0.3 0.0 9t.6 0.9 994r'..A
%2.061 2ffi @?w 0.4 0.4 0.0 n.0 ,0 12120.5
95 2.r19 2488 95332 0.4 0.4 0.0 n.3 ,0 [n50.3
96 2_220 2739 &757t 0.3 0.4 0.0 92.7 n826.0
97 23U 2212 &c783 0.3 0.4 0.0 93.0 Ata2
98 7.39t 2074 55 I 857 0.3 0.4 0.93.3 .2 14u2.6
I 2.48,.867 653724 0.3 03 0.93.5 1 1494d..3
100 2.576 860 65ssu 0.3 0.4 0.93.8 .3 t@2.7
l0l 2.673 757 657v1 0.3 0.4 0.94.1 .3 t75762
t02 2.775 694 659035 0.2 0.4 0.94.3 .4 18947.9
103 2.880 7A ffi|99 0.3 0.5 0.94.5 .5 22470.7
104 2.990 674 6r,2473 0.2 0.5 0.94.8 .6 23420.9
105 3.103 1450 66,3n4 0.2 0.5 0.95.0 .6 n694.4
106 3.D,t r606 665530 0.2 0.6 0.95.2 28114.4
107 3.34 1493 667U23 0.2 0.6 0.95.4 .8 29236;1
108 3.472 t347 668370 0.2 0.6 0.95.5 9 D513.2
r09 3.@4 1483 6698s3 0.2 0.7 0.95.8 2.1 36355.2
l0 3.74 l rro 67rc82 0.2 0.6 0.96.0 ,,1 33723.3
3.885 t360 672W 0.2 0.t 0.96.2 t.3 417s6.8
2 4.034 r06l 673502 0.2 0.6 0.96.4 2-4 16/,61.9
3 4.189 t249 674751 0.2 0.7 0.2 96.s 2.6 4W754
4 4.350 t20l 675963 0.2 0.8 0.2 96.7 2.8 51765.1
5 4.517 t234 677187 0.2 0.9 0.2 96.9 3.0 9W.2
6 4.691 nag 678396 0.2 0.9 0.2 97.1 3.2 65324.9
4.871 r008 6194{4 0.r 0.8 0.2 97.2 3.4 @9.2
8 5.059 r053 68fr''51 0.2 0.9 0.2 n.4 3.7 7tMs
9 s.236 r06l 681518 0.2 1.0 0.3 97.5 3.9 80621.8
120 5.462 r048 6n5ffi 0.l. t 0.3 97.7 4.2 894[3.2
l2l 5.677 953 6835 t8 0.1.0 0.3 97.8 4.6 9126f..5
r22 5.902 m0 6&1418 0.l.t 0.3 n.9 4.9 96878.3
t23 5.138 1!67 68528s 0.t. t 0.4 98.1 5.2 104978.6
124 6.383 799 686084 0.l.l 0.4 98.2 5.6 108842. I
t25 6.639 857 686941 0.1.3 0.4 98.3 6.1 t3t302.2
t26 69M 839 6gn8l 0.1.4 0.5 98.4 6.6 tM655.3
ln 7.179 787 688s68 0.t.4 0.5 98.5 7.1 t52416.3
128 7.4&731 689299 0.1.4 0.5 98.6 7.6 159238.5
t29 7.758 741 69m41 0.1.5 0.6 98.7 8.3 t8t262..6
30 8.061 7t6 69{J151 0.1.6 0.7 98.8 8.9 lo6/.32.9
8.372 651 691408 0.t.6 0.7 98.9 9.6 199981.5
32 8.690 591 69r998 0.1.5 0.7 99.0 10.3 2c296f,.3
33 9.016 535 g)534 0.1.5 0.7 99. I I 1.0 205413.9
34 9.347 s08 693U2 0..5 0.7 99.2 I 1.7 2t7057.t
35 9.82 488 69399 0..6 0.8 9.2 t2.5 2317M.9
36 10.020 v5 694tr15 0.I 1.0 9.3 t3.5 287320.s
37 10.36s 427 694sU 0.,6 0.9 9.4 t4.4 249138. r
38 10.720 387 6%889 0..5 0.9 9.4 15.2 249&8.3
39 084 337 69526 0.0 .4 0.8 9.5 16. I 240t37.5
140 458 329 695555 0.0 l_5 0.9 99.5 16.9 259328.2
l4l 841 324 69st79 0.0 1.6 1.0 99.6 17.9 28tW.9
t42 232 269 696148 0.0 1.4 0.9 9.6 18.8 2577t6.4
143 631 299 69ffi7 0.0 1.5 t.l 9.7 19.9 3 15589.4
t4 3.036 249 696tr,6 0.0 1.4 t.0 9.7 n.9 288656.2
145 47 l99 696895 0.0 t.2 0.9 99.7 21.7 2s2819.7
t4 863 ?36 697131 0.0 .6 l.l 99.7 D..9 3295&.8
t47 14.281 r53 6972U 0.0 l.l 0,99.8 ?i_7 233805.8
148 A.7n l4l 697425 0.0 1.0 0.8 99.8 24.5 2348r.0
149 r5. I l7 136 697561 0.0 l.l 0.8 99.8 25.3 245501-7
r50 r5.53 l 156 o77t6 0.0 1.3 t.0 99.8 26.3 305696.7
l5l 15.%3 153 697870 0.0 1.3 Ll 9.9 n.5 325308.4
59 of 80
this report conforns to pwbiors of 21 CFRpart 11 I'tB.zg2- SillE06- R.n 2 Ont. 2-3248- pct run reWl- 1Z1Z2VB14:@:4O- tuge 3 of 4
Channel Diamter
0un)
Counts
(#)
Crrmdafre
(#SDia)
Nun$er
e/n
Arce
CD
Volum
c/4
Numbr
(%sDie.)
Voluttb
(%SDia)
Ah, Volunr
ortP)
152 r6.3s3 90 697960 0.0 0.8 0.7 99.9 28.2 207183.3
153 t6.763 78 698038 0.0 0.7 0.7 9.9 28.8 lq2181.5
tv 17.176 75 6981 14 0.0 0.8 0.7 99.9 29.5 2m7t.2
155 17.595 65 698179 0.0 0.7 0.6 99_9 30. I 186384.0
r56 t8.0n 55 698234 0.0 0.5 0.5 99.9 30.7 t69483.4
t57 t8.62 50 698285 0.0 0.6 0.6 99.9 3r.3 t656y.6
58 r8.919 ffi 698345 0.0 0.7 0.7 99.9 32.0 2138%.3
59 t9j9 fi 598405 0.0 0.8 0.8 99.9 32.8 23059r.1
(fi r9.908 53 69M68 0.0 0.9 0.9 9.9 33.7 259593.3
6r 20.447 45 698513 0.0 0.6 0.7 9.9 4.4 2m51a.3
ta 21.015 20 598533 0.0 0.3 0.3 9.9 34.7 n7@.1
163 21.fi8 30 698563 0.0 0.5 0.5 100.0 3s.3 r593 18.9
t64 22.224 35 698599 0.0 0.5 0.7 100.0 36.0 2422..9
165 22.8fi 25 69844 0.0 0.4 0.5 100.0 36.5 157208.8
t6 23.512 ,<o8649 0.0 0.5 0.6 100.0 37.1 17t053.8
t67 24.|n t8 69867 0.0 0.4 0.4 r00.0 37.5 130192.2
168 24.U9 3 698669 0.0 0.1 0.1 100.0 37.6 20t93.5
r69 2s.s24 20 698689 0.0 0.4 0.6 lm.0 38.2 175058.3
170 26.2U2 5 698694 0.0 0.1 0.2 r00.0 38.4 47341.6
l7l 26.8m 8 698702 0.0 0.2 0.3 rm.0 38.6 76767.3
t72 27.591 20 6987n 0.0 0.5 0.8 100.0 39.4 22lr?3.8
t73 28.303 t5 698n7 0.0 0.4 0.6 100.0 40.0 179029.4
174 29.030 6 69874r'.0.0 0.2 0.3 100.0 40.3 96s8/..6
t75 29.n1 l3 698757 0.0 0.4 0.6 100.0 40.9 t73620.9
176 30.528 5 698762 0.0 0.2 0.3 100.0 4t.2 748U.9
t77 31.304 8 699n0 0.0 0.3 0.4 r00.0 41.6 121 105.4
178 32.W 13 69878? 0.0 0.4 0.7 100.0 4.3 2t7617.2
t19 32.9t6 l5 698Vvt 0.0 0.6 1.0 100.0 43.3 28t59.2
180 33.7s8 3 698800 0.0 0.1 0.2 100.0 43.5 s0626.7
l8l 34.47 10 6988r0 0.0 0.4 0.7 100.0 4.2 2t85s7.s
182 35.5n 25 698835 0.0 l.l 2.0 I00.0 46.2 s90r28.s
183 36.462 8 698U2 0.0 0.3 0.7 r00.0 46.9 t91397.2
184 37.436 J 69884s 0.0 0.1 0.2 100.0 47.1 69045.8
185 38.454 l0 698855 0.0 0.5 1.0 r00.0 48.2 29333.9
186 39.570 0 698855 0.0 0.0 0.0 100.0 48.2 0.0
187 &_a8 0 6988ss 0.0 0.0 0.0 100.0 48.2 0.0
188 41.7n 0 698855 0.0 0.0 0,0 t00.0 4.2 0.0
r89 42.954 J 698858 0.0 0.2 03 r00.0 48.5 tM2%.4
tm r4.fi4 J 698860 0.0 0.2 0.4 100.0 218.9 I l3zl4l.0
l9r 45.434 5 69886s 0.0 0.4 0.8 100.0 49.7 24859.t
192 46.736 3 698868 0.0 0.2 0.5 100.0 50.2 134342.0
193 48.080 0 598858 0.0 0.0 0.0 r00.0 50.2 0.0
l%49.467 3 698870 0.0 0.2 0.5 I00.0 50.8 159299.4
195 s0.900 3 698873 0.0 0.2 0.6 100.0 5l.3 t73546.8
t96 52.380 3 698&75 0.0 0.2 0.6 r00.0 s2.o t8s126.2
tn 53.907 3 698878 0.0 0.2 0.7 100.0 52.7 206t62.3
198 55.485 0 698878 0_0 0.0 0.0 r00,0 52.7 0.0
l99 57.n4 0 698878 0.0 0.0 0.0 I00.0 52.7 0.0
2U)58.795 0 698878 0.0 0.0 0.0 lm.0 9.7 0.0
20t 60.531 5 698883 0.0 0-5 2.0 100.0 v.7 583748.9
202 62.323 0 698883 0.0 0.0 0.0 100.0 v.7 0.0
203 4.t73 0 698883 0.0 0.0 0.0 r00.0 y_7 0.0
2U 6.0n 5 698888 0.0 0.8 2.6 100.0 57.3 759522.4
205 68.052 0 698888 0.0 0.0 0.0 rm.0 s7.3 0.0
206 70.086 0 698888 0.0 0.0 0.0 r00.0 s7.3 0.0
n7 72.1U 0 698888 0.0 0.0 0.0 I00.0 57.3 0.0
208 74.349 0 698888 0.0 0.0 0.0 100.0 57.3 0.0
2@ 76.582 0 698888 0.0 0.0 0.0 r00.0 57.3 0.0
210 78.885 0 698888 0.0 0.0 0.0 100.0 57.3 0.0
2n 81.260 0 698888 0.0 0.0 0.0 100.0 57.3 0.0
212 83.709 0 698888 0.0 0.0 0.0 t00.0 s7.3 0.0
60 of80
This report conforns to provisiors of 21 CFRpart 11 lv6lffi2- SIvEns- Rrn 2 Ont. 2-3248- pct rm rryl- 1Z1Z2AB 14:0O40- Pge4d 4
Channel DiatEter
fum)
Counb
(#)
Curmlatiw
(#sDia)
Nunter
v0
Arta
(w
Volum
(m
Number
(%SDia)
Vdum
(%Slxa.)
Ab.Volrre
tut)
213 85.233 0 698888 0.0 0.0 0.0 r00.0 57.3 0.0
2t4 88.834 0 698888 0.0 0.0 0.0 100.0 57.3 0.0
215 91.5t5 0 698888 0.0 0.0 0.0 100.0 57.3 0.0
216 91.276 0 698888 0.0 0.0 0.0 100.0 57.3 0.0
2t7 97. u8 0 698888 0.0 0.0 0.0 100.0 57.3 0.0
218 100.044 0 698888 0.0 0.0 0.0 100.0 57.3 0.0
2t9 103.052 0 698888 0.0 0.0 0.0 100.0 57.3 0.0
20 106.143 0 @8888 0.0 0.0 0.0 100.0 57.3 0.0
DI lw.322 0 698888 0.0 0.0 0.0 100.0 57.3 0.0
2n D.5n 0 698888 0.0 0.0 0.0 100.0 57.3 0.0
223 r5.9s6 3 698890 0.0 t.2 7.0 t00.0 4.3 2051813. I
224 9.418 0 698890 0.0 0.0 0.0 100.0 4.3 0.0
22s 22.9C2 0 698890 0.0 0.0 0.0 100.0 &.3 0.0
226 26.69 0 698890 0.0 0.0 0.0 r00.0 4.3 0.0
D7 30.438 0 698890 0.0 0.0 0.0 100.0 il.3 0.0
?28 34.341 0 698890 0.0 0.0 0.0 r00.0 &.3 0.0
n9 38.366 0 698890 0_0 0.0 0.0 100.0 il.3 0.0
230 142.522 0 698890 0.0 0.0 0.0 100.0 &.3 0.0
231 146.8r5 0 698890 0.0 0.0 0.0 100.0 4.1 0.0
Ltz 51.254 0 698890 0.0 0.0 0.0 100.0 64.3 0.0
233 55.845 0 698890 0.0 0-0 0.0 100.0 il.3 0.0
234 60.600 0 698890 0.0 0.0 0.0 t00.0 &.]0.0
235 6s.527 0 698890 0.0 0.0 0.0 100.0 &.3 0.0
236 70.638 0 698890 0.0 0.0 0.0 100.0 4.3 0.0
)11 75.945 0 698890 0.0 0.0 0.0 100.0 4.3 0.0
238 81.461 0 698890 0.0 0.0 0.0 r00.0 &.3 0.0
239 87.201 0 698890 0.0 0.0 0.0 100.0 &.3 0.0
24 193. l8l 0 698890 0.0 0.0 0.0 100.0 &.3 0.0
24t t*.346 3 598893 0.0 3.4 35.7 100.0 100.0 tu25269.1
242 205.022 0 698893 0.0 0.0 0.0 100.0 100.0 0.0
243 209.608 0 @8893 0.0 0.0 0.0 100.0 100.0 0.0
24 2t3.329 0 698893 0.0 0.0 0.0 100.0 100.0 0.0
245 2t6.67 0 698893 0.0 0.0 0.0 100.0 100.0 0-0
246 220.r99 0 698893 0.0 0.0 0.0 100.0 100.0 0.0
247 n4.6t4 0 698893 0.0 0.0 0.0 100.0 100.0 0.0
248 230.730 0 698893 0.0 0.0 0.0 100.0 100.0 0.0
249 239.503 0 598893 0.0 0.0 0.0 100.0 100.0 0.0
250 2s2.050 0 598893 0.0 0.0 0.0 r00.0 100.0 0.0
25r 269.670 0 698893 0.0 0.0 0.0 r00.0 100.0 0.0
252 294.551 0 598893 0.0 0.0 0.0 100.0 r00.0 0.0
253 329270 n 598893 0.0 0.0 0.0 100.0 100.0 0.0
2v 373.305 0 698893 0.0 0.0 0.0 100.0 100.0 0.0
255 423.030 0 698893 0.0 0.0 0.0 100.0 t00.0 0.0
256 474.M 0 698893 0.0 0.0 0.0 t00.0 100.0 0.0
61 of80
]t*s rcportconfcns toprorbbns of 21 CRpart 11 N.It,t [,62@- $m6- tun 3Qni. 2-&@-1?]12t2W 14:15:50- hgt I of 1
,A\ Pa rticle Technotogy Labs
tb€rBedryl-&t lvbdd.urboclL$
Fdocd:QnerdAn4Bb - Srrrdirl Sensor gN 186910
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ltis report confcrns to trorbirs cf 21 CRptrt 11 Vft t\,fl2@ - Sl,E)05 - Rn 3 Oil. 2 - 32@ - 12l12fNB 14:16:@.- RgE 1 d 1
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thb rwt confsm to pro/islYo of 21 CRpart 11 I'l6t202- S[,E)05- R.n 3 Gnt. 2-32.ffi- pct run rffi- 12l12lNA (:15:07 - Rge 1 d 4
,rN Particle Technology Labs
Qerdoc Becky l-hnibn
ma colectin daidt nFJ. 14:131Z12IM
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Cmnint ALLITACEIE{,EAL CnOA IIQ tr/6 Rrse tusijrc; F]t PIL; 615r-62' 526S9062 Bactgroud ocn6rirdi$: .t4.0 /llt
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10 0.532 1.211 &512
,0 0.673 1t.ll8 21.16
90 t.sD 3r2g 67.51I
C-hannel
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CtmuletirB
(#Slxa)
Nur&er(n
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vo
Volunr(n Nurter
(%sDtL)
Volum
(%SDl&)
AbcVdunr
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57 0.526 33971 $n1 7.4 OJ 0.0 7.4 0.0 2587.2
58 0.vt 3453 6U24 7.5 0.5 0.0 14.9 0.0 2907-9
59 0.563 25tm 93621 5.5 0.4 0.0 n.4 0.0 2358.8
(A 0.584 32123 125744 7.0 0.5 0.0 27.5 0,3345.4
61 0.606 30330 156075 6.6 0.5 0.0 y.1 0.3s29.3
a 0.49 28t52 tuDT 6.1 0.5 0.0 &.2 0,3675.2
63 0.655 30531 214857 6.7 0.6 0.0 6.9 0.4504.8
64 0.682 217qE 236r,56 4.8 0.5 0.0 3t;l 0.2 3624.1
6s 0.712 24065 2fi721 5.3 0.6 0.0 55.9 0.2 454r.8
6 0.74 5888 277ffi 3.7 0.5 0.0 60.6 0.2 3ffi.3
67 0.779 w2 295881 4.0 0.5 0.0 64.6 0.2 4515.4
68 0.815 5733 3l l614 3A 0.5 0.0 68.0 0.3 4*.2
o 0.852 3514 3?5128 3.0 0.5 0.0 71.0 0.3 4380.9
?0 0.w2 126 338328 2.9 0.5 0.0 73.9 0.3 40m.3
7t 0.932 9177 v1fis 2.0 0.4 0.0 15.9 0.4 3891.3
72 0.9n 9516 3S7r2l 2.t 0.4 0.0 '17.9 0.4 4580.0
73 .0ll 6733 3637ss {0.3 0.0 79.4 0.4 36/'8.7
74 .051 @76 370731 .5 0.4 0.0 80.9 0.4 4235.2
75 .090 5857 376597 .3 0.3 0.0 4.2 0.5 3n3.6
76 130 6200 3Wn 0.4 0.0 83.6 0.5 468s.4
77 170 4316 387103 0.9 0.3 0.0 84.5 0.5 3623.5
78 .2ll 44tr.2 391565 1.0 0.3 0.0 8s.5 0.5 4r53.8
79 .253 3931 395503 0.9 0.3 0.0 85.3 0.6 4056.0
80 .295 3272 395n4 0.7 03 0.0 87.1 0.6 3ru.3
8l 338 2986 401760 0;t 0.3 0.0 87.7 0.6 3748.0
a 382 3022 M7A 0.7 0.3 0.0 88.4 0.6 4116.9
s .427 2324 fin06 0.5 02 0.0 88.9 0.6 3535.3
u .413 N8 4m4il 0.5 0.2 0.0 89.4 0;1 393 t. I
85 .521 2494 41 1948 0.5 0.3 0.0 89.9 0;1 4592.4
86 570 1882 413830 0.4 02 0.0 00.3 0.7 3812.4
s7 t.621 t*2 415m 03 02 0.0 90.8 0.8 4330.0
88 t.614 t742 417514 OA 0.2 0.0 91.1 0.8 4280.1
89 1.730 1580 4t9[,4.0.3 o2 0.0 91.5 0.8 anl
E(l 1.788 1578 42M72 0.3 02 0.0 91.8 0.8 4726.6
64 of80
This reportcorfons to provislxs of 21 CFRpart 11 l\fin2.- St\,805- Rrn 3 &nt. 2-32m- pct run rry1- 1Z1Z2AB14:$:A7'We2d 4
Channel Diamter
(luD
CounB
(#)
CumulatitE
6SDia)
Nunber
en
Arte
fA
Vdunr
vt
Number
(%5Dia)
Volum
(%<Dia)
Ab.Vdu[*
(urf)
9l 1.850 399 422071 0.3 0.2 0.0 9.1 0.9 4ffi.3
n 1.916 360 423431 0.3 0.2 0.0 E2.4 0.9 5009.3
93 1.986 248 424tr78 0.3 0.2 0.0 92.7 0.9 5121.2
%2.061 380 42459 0.3 0.3 0.0 93.0 .0 6327.t
95 2.139 253 ann 0.3 0.3 0.0 93.3 .0 422.8
96 2.220 42U28 0.2 0.3 0.0 93.5 -0 6388.3
n 2344 a9v5 0.2 0.3 0.0 93.8 7153.9
98 2.391 t30 430675 0.2 0.3 0.0 %.0 8090.9
I 2.4U rm3 431679 02 0.3 0.0 94.2 .2 8030.4
100 2.576 1020 432ffi 0.2 0.3 0.%.5 a 9129.5
l0l 2.673 970 43366.9 0_2 0.3 0.%.7 J 9703.3
102 2.775 %7 434626 02 0.4 0.%.9 4 1u702.5
r03 2.880 890 4355r5 02 0.4 0.95.1 4 fit29.2
104 2.W &71 436386 02 0.4 0.95.3 .5 12187.5
105 3.103 n4 4372t1 o.2 0.4 0.9s.4 1.6 12901.3
106 3.271 839 438050 0.2 03 0.9s.6 1.7 t4692.9
t07 3.34 785 438835 02 0.4 0.9s.8 1.8 t5377.7
r08 3.472 765 439ffi 0.2 0.4 0.96.0 1.9 ta$.4
r09 3.M 114 4p03t5 0.2 OA 0.96.1 2.0 17sl 3.8
0 3.742 103 ,l4l0l8 0.2 0.5 0.96.3 2.1 1n94.3
3.885 638 44t656 0.1 0.5 0.96.4 2.2 I9589.5
2 4.034 sn 42238 0.1 0.5 0 96.s 2.4 20005.5
3 4.189 688 42926 0.2 0.6 0,96.7 2.5 26488.7
4 4.350 670 4/.3596 0.1 0.6 0 96.8 2;1 28851.7
5 4.5t7 601 444196 0.1 0.6 0.2 97.0 2.9 28C76.9
6 4.691 s82 M778 0.1 0.6 0.2 97.1 3.1 3tes.3
7 4.871 601 M5379 0.t 0.7 0.2 91.2 3.3 3649.9
18 5.059 5U 45903 0.0.7 0.2 97.3 3.5 35531.4
r9 5.X6 6t2 4r',6515 0.0.8 0.3 97.5 3.8 46503.0
20 s.4a 507 44742 0.0.7 0.3 9.6 4.1 43276.6
t2t 5.677 556 //7578 0.0.9 0.3 97.7 4.4 53250.9
t22 s902 556 4,4.8t34 0.0.9 0.4 91.8 4.8 59W.9
123 6.138 63 448596 0.0.8 0.3 97.9 5.1 56001.6
124 6.383 502 449@8 0.1.0 0.4 98.0 5.5 68326.6
t25 5.639 5il 4/,96f/9 0.t.l 0.5 98.2 6.0 78295.2
126 6.W 491 450100 0.l.l 0.5 98.3 6.5 84530.0
t27 7.1't9 4'.16 450575 0.1.2 0.6 98.4 7.t m49.8
t28 7.4&423 4509,9 0.t.l 0.6 98.5 y2182.5
129 7.758 36 45t3&0.l.l 0.6 98.5 8.2 8p373.7
130 8.061 388 45t752 0..2 0.7 98.6 8.9 r06389.8
l3l s.312 410 452t63 0..4 0.8 98.7 9.7 t2@,@.8
132 8.690 362 452524 0..3 0.8 98.8 10.4 124345.3
133 9.015 390 4529t4 0..5 0.9 98.9 n.4 t49576.7
34 9.347 358 453272 0.0.9 99.0 t2.3 53 I 05.6
r35 9.682 332 453ffi 0.5 t.0 99.0 13.3 57768,.7
136 t0.020 2n 453901 0..4 1.0 ts.r t4.2 s6232.s
37 10.365 263 45416/,0.A 0.9 9.2 t5.2 s3347.8
r38 10.720 287 454r''51 0..6 l.l 99.2 16.3 8526.t
139 I 1.084 267 4547t8 0..6 1.2 9.3 t7.5 r%177.3
llm I 1.458 229 4yyt7 0..5 l.t 99.3 18.6 180697.0
l4r I 1.841 297 455244 0.2.0 1.6 99.4 20.2 257785.6
t42 122i2 241 455485 0 7 1.4 99.4 21.6 230576.1
143 12.631 D6 455710 0.0 7 t.5 99.5 23.t 238137.7
t4 3.036 t73 4558&l 0.0 .4 1.2 99.s 24.3 20123 1.5
145 13.47 t79 45ffi3 0.0 .6 t.4 99.6 2s.8 D793.s
t46 13.863 r68 456231 0.0 .6 t.4 99.6 n.2 234165.5
147 t4.281 168 45639 0.0 7 1.6 99.6 28.8 2s5948.3
148 14.7fi 151 456550 0.0 ,6 1.6 99;1 30.3 25DA.t
149 15. r 17 |2 45ffi2 0.0 )1.2 99.7 3r.6 2A$2.1
150 15.53 I r08 456770 0.0 3 1.3 99.1 32.9 2nn3.9
l5t 15.%3 121 456893 0.0 1.5 1.6 9.7 34.5 2612U2.t
65 of 80
This report conforns to provisiors of 21 CFRpart 1'1 l\fi1212- SIVE005 - Rrn 3 6nt. 2-32169- post ru1 rry1- 12122U231415:A7 - IZge 3 of 4
Channel Diamter
fum)
Counts
(#)
Cumuladw
(#SDia)
Nunfter
vd
Arre
vd
Volurnc(n
Nun$er
(%-<Dia)
Volune
(%SDie.)
Ab"Vdum
Oufl
52 16.353 9r 45698r'0.0 7 .3 99.8 35.8 209274.2
53 t6.763 106 457Wr 0.0 .4 .6 *.8 37.4 2AXs.9
54 t7.176 86 457176 0.0 .2 .4 99.8 38.8 227ffi).9
55 7.595 73 457249 0.0 .J 99.8 40.1 207475.7
56 022 69 4573t8 0.0 3 99.8 4t.4 2l 1530.8
57 8.462 80 457398 0.0 .3 6 99.9 43.0 2(/.275.5
58 919 58 457456 0.0 1.0 .3 9.9 4.3 205029.8
s9 19.399 58 457514 0.0 t.l .4 99.9 45.7 221034.1
60 19.908 62 457575 0.0 1.2 6 99.9 47.2 254293.2
6l 20.47 52 457628 0.0 l.l .4 9.9 48.7 233779.5
62 21.015 32 457659 0.0 0.7 ,0 9.9 49.6 154085.4
63 2r.608 45 4577U 0.0 1.0 5 99.9 51.1 2l&63.7
64 n.n4 32 457736 0.0 0.8 I 9.9 9.2 1n229.4
t55 22.80 45 457781 0.0 l.l 7 99.9 53.9 n998.3
t6 23.5t2 26 457W7 0.0 0.7 I 99.9 55.0 t717n.0
t67 24.|n 2l 457827 0.0 0.6 0.9 r00.0 55.0 t5 I 826.3
168 24.U9 24 457852 0.0 4.1 t.2 100.0 57.2 194815.3
r69 2s.s24 r9 457U0 0.0 0.6 t.0 100.0 58.2 rc2Jn.3
t'70 26.202 22 457893 0.0 0.7 1.3 r00.0 s9.5 2t0822.2
t7t 26.890 l3 45't906 0.0 0.5 0.8 tm.0 60.3 132929.1
172 27.591 6 4579lL 0.0 0.2 0.4 100.0 o.7 6t536.7
t5 28.303 ll 4579n 0.0 0.4 0.8 r00.0 61.5 132859.2
74 29.030 4 457n6 0.0 0.2 0.3 100.0 61.8 477U.2
75 29.7'11 l9 457%5 0.0 0.8 .6 100.0 63.4 25769t.0
76 30.528 4 457949 0.0 0.2 0.3 100.0 61.7 55572.7
77 31.30{ll 4579fi 0.0 0.5 t.l r00.0 64.8 t7974tr,.7
78 32.W 4 457963 0.0 0.2 0.4 100.0 65.2 6/'598.2
79 32.916 6 457969 0.0 0.3 0.6 100.0 6s.9 l@488.5
80 33.758 6 457y75 0.0 0.3 0.7 100.0 6.6 n27|L.6
8l 34.627 6 457980 0.0 0.3 0.8 100.0 67.3 Dta,.0
182 35.527 4 4579U 0.0 0.2 0.5 lm.0 6'7.9 n'n.9
183 36.462 6 457sDO 0.0 0.4 0.9 100.0 68.8 142030. I
184 37.436 7 4579D7 0.0 0.5 1.3 100.0 70.0 2M957.9
185 38.4v )4579B9 0.0 0.1 0.3 t00.0 70.4 55534.5
r86 39.s20 9 458008 0.0 0.7 t.9 r00.0 72.2 301401.2
t87 &.628 0 458008 0.0 0.0 0.0 r00.0 72.2 0.0
188 4t.772 4 458012 0.0 0.3 0.9 100.0 73.1 14236,.0
189 42.954 6 4s8018 0.0 0.5 1.4 100.0 74.5 232t95.6
lm 4.t74 6 4s8m,3 0.0 0.5 1.6 100.0 76.1 252556.6
l9l 45.434 2 4sw25 0.0 0.2 0.6 100.0 76.7 9rs98.l
tn 46.736 0 458025 0.0 0.0 0.0 r00.0 76.7 0.0
r93 48.080 6 45803 I 0.0 0.6 2.0 t00.0 t6. I 32s637.4
194 49.457 2 458032 0.0 0.2 0.7 100.0 79.4 l{211.4
195 50.900 2 458034 0.0 0.2 0.8 100.0 80.2 l.287n.5
t96 52.380 0 458034 0.0 0.0 0.0 100.0 u.2 0.0
rn s3.fil 2 458036 0.0 0.3 0.9 r00.0 8l.l t52W.8
198 5s.485 4 458040 0.0 0.6 2.1 r00.0 83.2 333643.8
t99 57.n4 2 4580r'.2 0.0 0.3 l.l 100.0 u.3 181948.0
200 58-795 2 458044 0.0 0.3 1.2 100.0 85.5 t9u96.6
201 60.53 r 2 458046 0.0 0.3 1.3 100.0 85.9 21ffi2.5
za 62.323 0 4s8046 0.0 0.0 0.0 100.0 86.9 0.0
203 &.173 0 458046 0.0 0.0 0.0 r00.0 86.9 0.0
2U 6.082 2 458M7 0.0 0.4 t.7 r00.0 88.6 281824.0
205 68.052 ')458049 0.0 0.4 1.9 t00.0 90.5 307795.5
206 70.086 2 45805 0.0 0.4 2.t 100.0 92.6 33622r.5
207 72.\U 0 45805 0.0 0.0 0.0 100.0 9.6 0.0
208 't4.v9 0 4s805 0.0 0.0 0.0 r00.0 92.6 0.0
28 76.5n 0 45805 0.0 0.0 0.0 100.0 c2.6 0.0
2t0 78.885 0 45805 0.0 0.0 0.0 100.0 v2.6 0.0
2il 8r.260 0 45805 0.0 0.0 0.0 t00.0 n.6 0.0
2t2 83.709 2 458053 0.0 0.6 3.5 100.0 96. r 51?85s.7
66 of 80
This report confonrs to provbions of 21 CFRpart 11 lVEl2V2- SIVE0O5 - tun 3 ftr,t. 2-32469- pmt run report - 1212129?314:15:N - W4 d 4
Channel Diapter
Gtn)
C.otma
(#)
Cumdadw
(#Slxa.)
Nunfrer
v0
AIra
(v0
Volume(n Nunter
(%SDia.)
Volum
(o/o3Dit\
Ab6, Volurr
(tr#t
213 86.233 2 458055 0.0 4.7 3.9 rm.0 100.0 626255.3
2t4 88.834 0 458055 0.0 0.0 0.0 100.0 r00.0 0.0
2t5 91.5 t5 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
2t6 94.276 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
217 97.1 r8 0 458055 0.0 0.0 0.0 r00.0 100.0 0.0
218 100.044 0 458055 0.0 0.0 0.0 r00.0 100.0 0.0
219 103.052 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
220 106.143 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
221 tw3n 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
222 nsn 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
221 15.956 0 4580s5 0.0 0.0 0.0 100.0 r00.0 0.0
224 19.418 0 458055 0.0 0.0 0.0 t00.0 100.0 0.0
225 22.9n 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
226 25.654 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
227 30.438 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
n8 34.y|0 4s8055 0.0 0.0 0.0 100.0 100.0 0.0
229 38.366 0 458055 0.0 0.0 0.0 100.0 1003 0.0
230 0.s22 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
23t 46.815 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
232 51.254 0 458055 0.0 0.0 0.0 100.0 r00.0 0.0
233 s5.u5 0 458055 0.0 0.0 0.0 100.0 00.0 0.0
234 60.600 0 458055 0.0 0.0 0.0 100.0 00.0 0.0
235 65.527 0 458055 0.0 0.0 0.0 100.0 00.0 0.0
236 70.638 0 458055 0.0 0.0 0.0 r00.0 m.0 0.0
237 75.945 0 4s805s 0.0 0.0 0.0 100.0 00.0 0.0
238 81.461 0 458055 0.0 0.0 0.0 100.0 00.0 0.0
239 r87.201 0 458055 0.0 0.0 0.0 lm.0 00.0 0.0
2q 193. l8l 0 458055 0.0 0.0 0.0 100.0 00.0 0.0
24t t99.34 0 458055 0.0 0.0 0.0 100.0 00.0 0.0
242 205.0n 0 458055 0.0 0.0 0.0 100.0 r00.0 0.0
243 aCE.fi8 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
24 2t3.329 0 458055 0.0 0.0 0.0 100.0 t00.0 0.0
24s 2t6.67 0 4s8055 0.0 0.0 0.0 100.0 100.0 0.0
246 220.199 0 458055 0.0 0.0 0.0 100.0 r00.0 0.0
247 224.6t4 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
248 230.n0 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
249 239j03 0 458055 0.0 0.0 0.0 r00.0 100.0 0.0
250 2s2.050 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
251 269.670 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
252 294.551 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
253 329.270 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
254 173.305 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
255 423.030 0 4s8055 0.0 0.0 0.0 100.0 100.0 0.0
256 474.M 0 458055 0.0 0.0 0.0 100.0 100.0 0.0
67 of 80
'lt*s report mnfans to provbin d 21 CFRport 11 NM 1ri6 Acdqr Ela* - 32458 - 12l12fXB 14:km - m0 1 d I
lvbddnnberLflO
SerEor 9N 186010
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lN Particle Technology Labs
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il0ol Heflire: 1 2121a,3., 1 4:8
Win Flaane 18601oPTL ((2-2&23)
Ofinr* ,\tr-hACElEtdfrALmA [q il/6 RrEe tusir.q Ft PIU 6157'64 ffi1{2
Nbdx0.836gn
Irib&0.e6lrn
I\bdrr0.665l,n
Smdad bvEiirr 1.150pn
Slovress:21.8 pn
l(r$is:841.'l gttt
FLillvdurs 60.0 nl
SamleTfis 60 sec
ergeOs-{olln DMimhctdl.858'PrGhddOSEn RoEF: 1.S
Charnds:1$ Bad€rqnd:20ffi
Totdorrrts:35-/861 OilrilJrL:71tl3#rL
M5 Acetone Blank - 32d58
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68 of 80
{httn1 t?'t1
lhis ruport conforns to pwisirr d 21 CtRpdt 11
A\ Pa rticle Technology Labs
L,becBeclryFmUt
mocd: GErEral Ardilsb - Srrrciiqt
Rn Edlrra: 12121X814:27
Fbpod Ha|fnE: 1Z12IXB, 14:N
QnIIIAuI\ACEIEIIqLGFOA [q i/ERrB6*siX.q Rt PTL; fi'rr{A 52m1-@
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Vft tr,EAcetrrffi-32458- 1Z12|XB1429"14- m01d 1
lrbaft42S01rn
lr/b&94.26lm
lvbdan:364@gn
Sardnd BlrtiioE n.753tm
Slelvrrss:0.6pn
l(tbb:-O91m
RilVdure:60.0r1
SardeTirB:60ss
Rarpeo.s-4mlm Ohdonhr:1.858
llreMd0.5t,n RoEF1.O
Ctmneb:1S Badgtq1dzo#d
TdJQr*357863 GrtJnL715/3#nl
M5 Acrlone Blank - 32158
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69 of80
Ihb report cqrfons to pwblrs of 21 CRpart 11 lv6Acetane Bark - 3458 - pct rtn re4rrl - 12l 1Z2W14:28:36 - Rge 1 of 4
fumt C€rerd ArCysis - Srnrstin
lvbdd# LEl00
SerEaSAt 1805910
Sersc node: Srrnatitt
Qbr&t file: 180691GPI1 (m-2&23)
Gbration &tetirB: @-2&23
Sarple ffiodrliott ttrhnd
VdlrrDsanpled: 60.0nL
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Qerator Beclvl-hrrfltdr
Oda cdlec{ifi daldtinei 14:27 121 Qr2WJ
QctHdline: 142d)1AQ2W
Targetcdlcenfdtoft 7m
Sanfle: lv6Acetre Blak- 32rL58
ernio[ALJ-IMCEIE+EALGRSP, LLC tv6RrseFbsidt"E; FH Prl; 615r/-@; P6991-@t**ror.ndcrunrratinr:2o/nl
&rlts necued 19618 - Surna[imvdtage i0.6V
Tdal cdrts (> 0.5 tro, ryry . &tinclim vd&: 1 0.6 V
Tdd carns/nl. (> 0.5 prrf:715/3/nL
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DN DA DV
10 0.528 0.675 t2.2@
50 0.643 12.036 36.24
90 t.052 43.W7 9t.y)t
(}anrel Diemtor
(rr,
CounB
(#)
CwmledrB
6sllla.)
Nur*er(n Arca
an
VolunE
(m
Nunter
(%SIx&)
Volutr
(%!IDe)
Atf,,Volm
(urfi
57 0.526 31783 31783 8.9 .2 0.0 8.9 0.0 2420.5
s8 o.w 3073s 62sn 8.6 3 0.0 17.5 0.1 25%.1
59 0.563 ?24r,2 umr 6.3 .0 0.0 23.7 0.1 29t.2
@ 0.584 28r'.78 I 13398 8.0 3 0.0 3t.7 0.1 2965.8
6l 0.606 2&43 1fi241 7.5 .4 0.0 10,0.2 3123.4
62 0.629 24859 165100 6.9 .4 0.0 216.1 0.2 3245.2
63 0.655 267@ 191809 7.5 .6 0.1 s3.6 0.3 3928.0
&0.682 18796 210605 5.3 2 0.0 s8.9 0.3 ,t24.9
65 0.712 2c,94 23t59E 5.9 1.5 0.1 64.7 0.4 39A.2
6 0.74 t4s32 246132 4.1 l.t 0.0 68.8 0.4 3l32.6
67 0.779 15898 2f20B0 4.4 1.3 0.t 73.2 0.5 3m8.7
58 0.815 t3252 ns2g2.3.")t.2 0.r 76.9 0.5 3751.9
@ 0.852 11274 286556 3.2 1.1 0.1 80.1 0.6 3654.8
70 0.89 11101 29'.7657 3.1 1.2 0.1 83.2 0.7 4121.0
7l 0.932 7170 304826 2.0 0.9 0.0 85.2 0.7 3&10.1
72 0.972 7171 311998 2.0 0.9 0.0 n.2 0.8 y,51.4
73 1.011 4n2 316969 1.4 0.7 0.0 88.6 0.8 269d.0
74 .051 4929 321898 1.4 0.8 0.0 90.0 0.8 292.5
75 .090 3820 325'lt8 Ll 0.5 0.0 91.0 0.9 2s91.6
76 130 36m 329Q8 t.0 0.7 0.0 9.0 0.9 278&4
71 170 2633 332041 0.7 0.5 0.0 n.8 0.9 2210.2
78 .2|24'13 334513 0.7 0.5 0.0 93.5 .0 23M.3
79 .253 2457 336570 0.6 o.4 0.0 94.0 1.0 21 18.6
80 .295 1650 i8n0 0.5 0.4 0.0 94.5 1.0 tw1.t
8l .338 1486 $n6 0.4 0.4 0.0 %.9 r865.5
n .382 t3'79 341085 0.4 0.4 0.0 95.3 Im5.6
83 LAn I 133 yDrS 0.3 0.3 0.0 95.6 1724.0
u t.4'13 I 109 vBn 0.3 0.3 0.0 95.9 1856.7
&5 1.521 1045 w373 0.3 0.3 0.0 96.2 1.2 192;6.2
86 1.570 ta6 v539E 0.3 0.3 0.0 96.5 t2 2U7.5
ct t.621 938 3fi337 0.3 0.3 0.0 96.8 1.2 2cf13
88 t.674 717 34745r'.0.2 0.3 0.0 n.0 3 1761.9
89 1.730 54t y759s 0.2 0.2 0.0 v7.t 1.3 1465.4
90 1.788 674 va69 0.2 0.3 0.0 9.3 1.3 20,;0.t
70 of 80
Ctannel Dianrter
0un)
C.ounG
(.#)
GmruIatiw
(#<Dir.)
Nun&er(o
Area
e/t
Vdunr
(v)
Nunter
(%SDia.)
Vdurr
(%sI)iL)
Ah.Vdum
tprfl
9l 1.850 529 34U99 0.0.3 0.0 97.5 3 1756.4
n 1.916 494 349293 n 0.3 0.0 n.6 4 1820.6
93 1.986 437 34n30 0.0.2 0.0 97.7 4 t791.9
94 2.061 500 350229 0.0.3 0.0 97.9 4 D91.0
95 2.139 412 350(r'.2 0.0.3 0.0 98.0 .4 2l 13.5
96 2.n0 314 350956 0.0.2 0.0 98.r .5 1798.3
97 2.3U 359 35r314 0.0.3 0.0 98.2 1.5 2296.0
98 2.391 359 3s1673 n 0.3 0.0 98.3 t.5 256r,.7
I 2.4U 297 351n0 0.0.3 0.0 98.4 1.6 2378.8
100 2.576 277 39247 0.0.3 0.0 98.4 t.6 2477.0
l0l 2.673 277 352524 0.0.3 0.0 98.5 t.7 27@.4
tm 2.775 273 3521n 0.0.3 0.0 98.6 t.7 3054.8
103 2.880 277 353074 0.0.3 0.0 98.7 t.7 w2.7
104 2.990 l9 353273 0.0.2 0.0 98.7 t.8 2781.4
105 3.103 235 3535@ 0.0.3 0.1 98.8 1.8 3692.3
r06 3.221 232 t53741 0.0.3 0.t 98.8 1.9 Q65.3
107 3.y4 2A 354003 0.0.4 0.1 9&9 2.0 5130.0
108 3.472 r80 354183 0.0.3 0.1 99.0 2.0 3}l8.0
r09 3.&2U 3543&7 0.0.4 0.99.0 2.1 s010.3
l0 3.742 t3'7 3v525 0.0 0.3 0.1 99. I 2.2 3TD.3
3.885 149 3ga3 0.0 0.3 0.1 99.1 2.2 45il.3
112 4.034 124 354198 0.0 0.3 0.t 99.t 2.3 4n9.2
3 4.189 t37 3v935 0.0 0.3 0.1 99.2 2.4 5291.2
l14 4.350 ill 1550r'-7 0.0 0.3 0,9.2 2.4 4803.0
5 4.5r7 150 355197 0.0 0.4 0.99.3 2.5 72fi.6
l6 4.691 ll9 3553 l6 0.0 0.4 0,99.3 2.5 42s.0
7 4.gil 125 35543 0.0 0.4 0.99.3 746.2
8 5.059 ll5 355558 0.0 0.4 0 9.4 2.8 7810.2
l9 5.256 il3 355671 0.0 0.4 0 9.4 3.0 8614_4
t20 5.462 93 355164 0.0 0.4 0.99.4 3.1 7E24.0
t2t 5.6n 89 355853 0.0 0.4 0.9.4 17 8543.6
t22 5.902 85 355939 0.0 0.4 0.99.5 3.3 9201.5
t23 6.138 74 35@13 0.0 0.4 0.99.5 3.5 89E7.0
t24 6.383 80 356093 0.0 0.5 0.2 99.s 3.6 10879.1
t2s 6.639 69 3silA 0.0 0.4 o.2 99.5 3.8 l053 l. l
t26 6.m4 n 35449 0.0 0.6 0.2 99.s 4.0 t5u6.7
127 7.t79 78 356327 0.0 0.6 0.2 9.6 4.2 l5 I 17.9
t28 7.4&65 3s6392 0.0 0.5 0.2 9.6 44 14t57.3
129 7.758 78 3s(470 0.0 0.6 0.3 9.6 4.7 t9076.2
130 8.06r 56 3s696 0.0 0.5 0,2 9.6 4.9 1528r'..3
t3l 8.372 67 356593 0.0 0.6 0.3 9.6 5.2 N*7.0
132 8.690 54 ,5&6 0.0 0.6 0.3 99.7 5.5 18514.6
133 9.0r6 <t 3s@ 0.0 0.6 0.3 99.7 5.8 t99(n..2
134 9.347 43 35674t 0.0 0.5 0.3 9.7 6.0 tE268.7
135 9.682 6l 356803 0.0 0.8 0.4 D.7 6.4 29134.2
136 10.020 6l 3568er 0.0 0.9 0.5 9.7 6.9 32298.1
t37 10.365 45 356908 0.0 0.7 0.4 9.7 7.3 25989.1
t38 10.720 58 356966 0.0 0.9 0.5 9.7 7.8 37t47.2
139 OM 46 3570t2 0.0 0.8 0.5 99.8 8.3 331r7.0
140 t.458 52 357065 0.0 0.9 0.6 ts.8 8.9 40y72.5
t4t r.841 )t 3571U2 0.0 0.7 0.5 9.8 9.3 32298.4
142 2.232 45 357146 0.0 0.9 0.6 99.8 r0.0 4729.3
143 L63t 39 3571 85 0.0 0.9 0.5 99.8 10.6 4n57.2
t4 3.036 30 1572t5 0.0 0.7 0.5 99.8 r 1.0 wu.3
t45 3.47 4l 357?56 0.0 .0 0;1 99.8 I 1.8 520/'3.1
t46 3.863 39 357295 0.0 .0 0.8 99.8 t2.6 w23.8
t47 4.281 39 357334 0.0 t 0.9 99.9 13.4 5949& r
148 4.7m 37 3s731t 0.0 I 0.9 w.9 14.3 61796.6
149 15. I 17 26 357397 0.0 0.8 0.7 9.9 15.0 470r'.8.4
150 I 5.531 37 357434 0.0 1.2 1.0 99.9 16.0 n8v2.9
l5l 5.943 24 357458 0.0 0.8 0.7 9.9 r6.8 5t246.6
Ihis report confornB to proil/isiors of 21 CFRpart 11 [tE Acetone Bank - 32458 - pct rm te{rll - 1Z 12l2AB fi:28.:.ffi - W 2 d 4
7l of80
Channel Dirnrter
(rtm)
Counts
(#)
Cunrulatir,e
65Dta)
Nunter
vd
Area
v0
Volunr
(v)
Number
(ohSDia.)
Vdum
(%<Dta)
AbcVolum
(unf)
ts2 r6.353 t9 3574n 0.0 0.7 0.6 99.9 17.4 a*t.l
153 t6.763 r3 35749{)0.0 0.5 0.5 99.9 t7.9 32077.8
154 t7.176 l9 3575@ 0.0 0.8 0.7 99.9 r8.6 49296.9
155 t7_595 22 35753 l 0.0 t.0 0.9 9.9 19.5 63587.6
r56 t8.on 24 357s55 0.0 Ll Ll 99.9 20.5 74f.29.4
157 18.462 ll 357566 0.0 0.5 0.5 9.9 2l.l 36730.6
rs8 18.919 'r',357588 0.0 t.l 99.9 D..2 79054.3
159 19.399 24 357613 0.0 1.3 3 9.9 23.5 92327.5
160 19.908 24 357637 0.0 1.3 .4 99.9 ?5.0 9D'182.2
r61 m.M7 l9 35'7655 0.0 l.l 7 9.9 26.2 83|6/..4
IO 21.0r5 l3 357668 0.0 0.8 0.9 99.9 27.1 63197.4
163 21.608 ll 3s7679 0.0 4.7 0.8 9.9 27.9 58883.5
t&1) ))A 7 357696 0.0 Ll 1.4 100.0 29.3 96095.0
165 2Z8Q l3 35n49 0.0 0.9 1.2 100.0 30.5 81345.0
t6 23.5t2 3 357n2 0.0 1.0 1.3 100.0 31.8 88514. I
167 24.t77 7 $7n0 0.0 0.6 0.8 100.0 9.5 5r'982.5
168 24.U9 9 357',l39 0.0 0.8 l.t 100.0 33.6 74634.3
169 25.524 6 357745 0.0 0.5 0.7 100.0 v.3 48525.5
170 26.24 tl 3s17s6 0.0 t.l 1.5 100.0 35.8 1M9D6.6
171 26.8n 1 357763 0.0 0.7 l.l 100.0 36.9 75660.8
177 27.591 4 357767 0.0 0.4 0.6 r00.0 37.5 40861. l
113 2&303 il 351n8 0.0 t.2 t.9 100.0 39.4 132336.7
t74 29.030 6 35178/ 0.0 0.6 t.0 100.0 40.4 71394.4
175 29.771 6 35n89 0.0 0.7 Lt 100.0 41.5 nN3.3
t76 30.528 4 357793 0.0 0.5 0.8 100.0 4.3 55354.2
177 31.304 0 35n93 0.0 0.0 0.0 100.0 42.3 0.0
178 32.W 9 357ffi2 0.0 1.3 2.3 100.0 44.7 160860.s
179 32.916 6 357808 0.0 0.8 1.5 100.0 6.2 twn.7
180 33.758 6 357813 0.0 0.9 1.6 lm.0 47.8 I t2268.3
l8r 34.O7 0 357813 0.0 0.0 0.0 100.0 47.8 0.0
tn 35.527 4 3s7817 0.0 0.6 1.3 r00.0 49.0 87243.4
t83 16.462 4 3s7nt 0.0 0.7 1.4 100.0 fi.4 %3t4.4
t84 37.436 6 357r/i6 0.0 l.l 2.2 100.0 52.6 r53l13.9
85 38.454 2 357828 0.0 0.4 0.8 100.0 s3.4 55316.2
186 39.520 9 157837 0.0 2.0 4.3 100.0 57;l 300216.0
u q.628 0 35783'l 0.0 0.0 0.0 100.0 37.7 0.0
88 41.772 0 3578J7 0.0 0.0 0.0 100.0 57.7 0.0
89 42.954 7 3578r',5 0.0 1.9 4.4 r00.0 62.1 308376.7
190 4.t74 2 3578r'.7 0.0 0.5 t,2 100.0 63.3 83854.5
l9l 45.434 0 3578r'.7 0.0 0.0 0.0 100.0 63.3 0.0
ln 46.736 0 3578r'.7 0.0 0.0 0.0 100.0 63.3 0.0
193 48.080 2 3s7U9 0.0 0.6 1.6 100.0 4.9 l08l 19.0
l94 49.467 4 157852 0.0 1.3 3.4 100.0 68.3 235s05. r
%s0.900 2 3578s4 0.0 0.7 1.8 100.0 70.1 t2828r',.t
96 s2.380 0 357854 0.0 0.0 0.0 100.0 70.t 0.0
n 53.907 2 357856 0.0 0.7 2.2 r00.0 72.3 ts2396.2
98 55.4E5 0 357856 0.0 0.0 0.0 100.0 n.3 0.0
I 57.n4 0 357856 0.0 0.0 0.0 100.0 72.3 0.0
ZN 58.795 0 357856 0.0 0.0 0.0 100.0 72.3 0.0
20t 60.531 0 357856 0.0 0.0 0.0 100.0 n.3 0.0
202 62323 0 357856 0.0 0.0 0.0 100.0 n.3 0.0
203 9.173 0 357856 0.0 0.0 0.0 lm.0 n.3 0.0
2U 6.0n 2 357858 0.0 l.l 4.0 100.0 76.4 280715.8
205 68.052 2 357860 0.0 t.2 4.4 100.0 80.8 306585.2
206 70.086 0 3578r0 0.0 0.0 0.0 100.0 80.8 0.0
207 72.tU 0 357860 0.0 0.0 0.0 r00.0 80.8 0.0
208 't4.349 0 357860 0.0 0.0 0.0 100.0 80.8 0.0
2@ 76.5n 0 357860 0.0 0.0 0.0 r00.0 80.8 0.0
210 78.885 0 357860 0.0 0.0 0.0 r00.0 80.8 0.0
2tl 81.260 2 35'r'.i6z 0.0 l1 ?.5 100.0 88.3 52t977.8
212 83.7@ 0 357862 0.0 0.0 0.0 100.0 88.3 0.0
'lhb report mnforns to provisions of 21 CFRpart 11 tv6Acetone Bank - 32458 - pct run reprll - 121?J2gn M:fr'.% - Hge 3 cf 4
72 of 80
Clurnel Diamtsr
0m)
Crilnts
(#)
Cumuladw
(#Slxa.)
Number(o
Ama
vc
Volume
(v)
Nunter
(%SDie)
Volum
(%SDia.)
Ab.Volurr
rprft
2t3 86.233 0 357862 0.0 0.0 0.0 t00.0 88.3 0.0
2t4 88.834 0 357t!52 0.0 0.0 0.0 100.0 88.3 0.0
215 91.515 0 3s7%2 0.0 0.0 0.0 100.0 88.3 0.0
2t6 %.276 2 357863 0.0 2.3 |.7 100.0 r00.0 8l5l 10.6
217 11897 0 3s7863 0.0 0.0 0.0 100.0 100.0 0.0
218 r00.044 0 357''fi3 0.0 0.0 0.0 100.0 100.0 0.0
2t9 r03.052 0 1s7K3 0.0 0.0 0.0 100.0 100.0 0.0
n0 t06.143 0 357863 0.0 0.0 0.0 100.0 100.0 0.0
nt tw3n 0 357863 0.0 0.0 0.0 100.0 100.0 0.0
))1 n2.592 0 3578r.3 0.0 0.0 0.0 100.0 100.0 0.0
223 l 15.956 0 357863 0.0 0.0 0.0 100.0 100.0 0.0
224 I19.418 n 357863 0.0 0.0 0.0 100.0 100.0 0.0
225 122.982 0 357t]tr,3 0.0 0.0 0.0 100.0 00.0 0.0
226 t26.6v 0 357f]r,3 0_0 0.0 0.0 100.0 00.0 0.0
D7 130.438 0 357863 0.0 0.0 0.0 100.0 00.0 0.0
228 t34.yt 0 357863 0.0 0.0 0.0 100.0 00.0 0.0
29 138.366 0 357863 0.0 0.0 0.0 1m.0 00.0 0.0
230 t42.522 0 357863 0.0 0.0 0.0 r00.0 00.0 0.0
23r 146.8r5 0 357863 0.0 0.0 0.0 100.0 r00.0 0.0
232 15t.254 0 3578tr,3 0.0 0.0 0.0 100.0 100.0 0.0
213 155.845 0 357tX3 0.0 0.0 0.0 100.0 100.0 0.0
234 160.600 0 3578tr,3 0.0 0.0 0.0 100.0 100.0 0.0
23s 165.97 0 3s7863 0.0 0.0 0.0 lm.0 100.0 0.0
236 170.638 0 357tb3 0.0 0.0 0.0 r00.0 r00.0 0.0
237 t75.945 0 357863 0.0 0.0 0.0 100.0 100.0 0.0
238 l8l.46l 0 3571K3 0.0 0.0 0.0 100.0 100.0 0.0
?39 187.20r 0 357853 0.0 0.0 0.0 100.0 100.0 0.0
24 193. l 8l 0 357863 0.0 0.0 0.0 100.0 100.0 0.0
24t t99.46 0 357863 0.0 0.0 0.0 r00.0 100.0 0.0
242 20s.un 0 357t]63 0.0 0.0 0.0 100.0 100.0 0.0
243 2@.&8 0 357',t363 0.0 0.0 0.0 100.0 100.0 0.0
24 213-329 0 357863 0.0 0.0 0.0 100.0 100.0 0.0
245 2t6.#7 0 3s7863 0.0 0.0 0.0 100.0 t00.0 0.0
246 220.19 0 3s7863 0.0 0.0 0.0 100.0 100.0 0.0
247 224.614 0 357863 0.0 0.0 0.0 r00.0 r00.0 0.0
248 230.730 0 157863 0.0 0.0 0.0 r00.0 100.0 0.0
249 L19.503 0 3571]r,3 0.0 0.0 0.0 100.0 t00.0 0.0
250 252.050 0 357863 0.0 0.0 0.0 100.0 r00.0 0.0
25t 269.670 0 3578r,3 0.0 0.0 0.0 r00.0 100.0 0.0
252 294.551 0 357853 0.0 0.0 0.0 100.0 100.0 0.0
253 329.270 0 3s7863 0.0 0.0 0.0 100.0 100.0 0.0
2v 373.305 0 357863 0.0 0.0 0.0 r00.0 r00.0 0.0
255 a3.030 0 357863 0.0 0.0 0.0 100.0 100.0 0.0
256 474.M 0 357863 0.0 0.0 0.0 100.0 100.0 0.0
Ihb report mrforns to Fovisiors of 21 CFRpart 11 Iv6AcetoneBank- 32458- pctrm tryl- 1Z12l2gA 14:28:36- @e4d 4
73 of80
74 of 80
plltffiipe
TECHN:CAL GROUP QA/QC Data
Locstion Rio Tinto Kennecott - Magna, UT
Source Flash Smelting Furrace Dry Feed Bin Baghouse SME005
Project No. AST-2023-3179
Parameter PM
DrtP Noz-zle II)#l #2
tameter (tn,,
#3 Dn (Averase) Difference Criteria Mat€riAl
10t)4t)1 3 I 79-t 0lt0 03r0 0 310 0 310 0 000 < 0.004 in.glos
Date Pitot ID dnmrpe?misrlisnment?
caltbratrcn or
R.noir ra^nir.d,
10/24/23 3 I 79-1 no no no
Dnte Probe or
TLa,m^.^rnta rn
Reference Indicated Difference Criteria Probe Length
t0/24t23 3179-l 50.0 50.0 o ooa + 1.5 % (absolute)3
Field BalAnce Check
Date 10t24t23 10125123
Balmce ID 542881026 5A2881026
Certified Weight ID sLc-1KG-3 sLc-1KG-3
Certified Wdght (g)1000.0 1 000-0
Meaured Weight (g)1000.0 lmo-o
Weight Differene (g)0.0 0.0
Date Barometric Evidence of Reding Verified LAIDrAllOn Or
D- -i- --^-i--it Weather Ststion Location
t0t24/23 Weather Station NA SALT LAKE CITY,UT
Drte Meter Box ID Positive Prqsure Leak Check
10t24/23 MB.3O Pass
Reagent Lot#l'ield Prep
nerformed Field Lot Date By
ACETONE 230520
HEXANES 2183s9
DI 231106
75 of80
i:AIlme
s.tJqct rrsr \(;
DGM Calibration-Orifi ces
Document lI 620.004
Revis or 22.3
Effectve Dat 12/16/22
lssulng Department Tech Serylces Paq(1of1
Equipment Detail - Dry Gas Meter
Console lD. lV5-30
Meter 5/N N/5-30
Critical Orifice 5/N: '1330
Calibration Detail
nitial Barometric Pressure, in. Hg (Pb)
:inal Barometric Pressure, in. Hg (PbF)
\veraqe Barometric Pressure, in. Hq (Pb)
25.75
25.79
25.77
:ritifcal Orifice lD (Y)
K' Factor, ft3 R'/2 / ln. wc.min (K)
Vacuum Pressure, in. Hg (V,
nitial Dclvl Vo ume, ftr (vm )
Final DGN/ Volume, ft3 (Vmr)
Total DGN/ volume, ftr (vm)
1330-31
0.8429
13.0
4n.2AA
438.91 0
15.710
1330-31 '1330-25
0.6728
15.0
478.444
489.350
10.910
1330-2 5 1330-19
0.5186
r.a
512.800
522.710
9.910
1330-19
4.8429 0 673 0.5.19
13.0
438.914
454.t]zi
15.715
150
489.350
500.160
10.810
r.a
522.7rc
532.475
9 765
\mbient Temperature, "F (Ta)
nitial DGN/ Temperature, 'F (Im )
:lnal DGM Temperature, 'F (TmF)
\veraqe DGM Temperature, 'F ( Tm)
66
72
74
73
66
74
74
74
66
t5
75
75
66
75
75
75
66
74
73
14
66
1)
t3
73
Elapsed Time (O)
Meter Orlfice Pressure, in. WC (AH)
Standard Meter volume, ftr ftmstd)
Standard Critica Oriflce Volume, ft3 (Vcr)
l\leter Correction Factor (Y)
Jo erarce
Orifice Ca ibration Value (AH @)
To e.arce
O'ifice Cal Checl,
15.00
3.10
13 5251
14.2107
r 051
0.001
1.673
0 012
'15.00
3.10
'13 5040
14.2107
1.052
0 003
1.669
0.015
13.00
2.00
9.3284
9 8306
1.454
0.004
1.682
0.002
.13.00
2.00
9.2429
9.8306
1.064
0.014
1.682
0 002
15.00
1.24
8.4779
8.7433
'1.031
0.018
1 700
0.015
15 00
1.20
8.3617
8.7433
1.046
0.004
1.701
0.017
1.26 1.95 '1.91
Meter Correction Factor ff)1.050
3riice Calibration Value ( H @)1.685
Positive Pressure Leak Check Yes
Equipment Detail - Thermocouple Sensor
Reference Calibrator Make: Omega
Reference Calibrator Model: CL23A
Reference Calibrator S/N. T-197207
Calibration Detail
Reference Temp.Display Temp Accuracv Difference
"F t .F
0
68
100
464
q,R
560
2
68
100
462
(24
560
-0.4
00
0.0
2
0
0
223 683
708
731
225
250
275
685
71A
11C
-0.3
-0.3
-03
2
2
2
300
400
500
600
700
800
900
1,000
1,100
\204
760
860
960
1,060
'1,160
1,264
1,360
\464
1,560
'1,660
303
401
501
601
743
801
903
1,003
1,101
1,204
763
861
961
.r,061
1,163
1,261
1,363
1,463
1,561
1,664
-4.4
-0.1
-0.1
-0.1
-0.3
-0.1
-0.2
-4.2
-0.'1
-02
3
1
,1
1
3
1
l
3
't
4
Personnel
5/12/2023
76 of 80
Calibration By:
Calibration Date:
R. Burton
77 of 80
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80
RTKC Smelter Compliance Testing - Operations Assessment 1012020 - 1012023
DEPABTMENT OF
OUAUry
DEC ?A ?l:ti
Top 36 Dryer Ooeration Davs (Dailv Averaqes)
DATE Dryer Feed
STPH
259.4
252.4
250.4
248.3
246.9
245.4
243.0
241.8
240.9
240.0
239.9
239.2
239.2
239.2
238.9
238.9
238.9
238.6
238.5
236.9
236.0
235.7
235.4
235.2
234.9
234.4
232.5
232.1
231.8
231.0
230.8
230.8
230.5
230.1
230.0
229.9
238.3
2',14.4
February 22,2021
February 18,2021
March 17,2021
January 14,2021
January 7,2021
December 1,2020
March 31,2021
May 14,2021
February 21,2021
November 9,2020
January 10,2021
April1,2021
November 24,2020
October 25,2020
January 17,2021
December 30,2020
May 10,2021
November 22,2020
January 29,2021
February 11,2021
March 28,2021
January 26,2021
March 14,2021
December 25,2020
February 26,2021
July 26,2021
December 10,2020
November 14,2020
December 28,2020
July 23,2021
November 17,2020
November 5,2020
July 24,2021
February 17,2021
January 13,2021
November 15,2020
Average for 2023 test:
Minimum 90% to meet:
79 of 80
DIVISION OF AIR QUALITY
80 of80
Source Information
Division of Air Quality
Compliance Demonstration
Source Information
Company Name Kennecott - SME005
Company Contact:Jenny Esker
Contact Phone No.801-569-6494
Source Designation:SME005
Test & Review Dates
Test Date: 10/25/2023
Review Date: 1/9/2024 Tabs Are Shown
Observer:
Reviewer:Paul Morris
Particulate Emission Limits
lbs/MMBtu lbs/hr gr/dscf
1.250 0.016
Emission Rates - "Front Half"
lbs/MMBtu lbs/hr gr/dscf
0.0410 0.0025
Test Information
Stack_I.D._inches As ft^2 Y Dl H @ Cp Pbar Pq (static)Dn
17.50 1.67 1.0500 1.685 0.84 26.88 0.46
0.31
Contractor Information
Contracting Company: Alliance Technical Group, LLC
Contact: Shamit Nakra
Phone No.: 385-252-7553
Project No.:
Circular
10100
9780
9860
9190
8710
8710
8710
10540
10640
11950
320
10610
10200
10390
1970
1800
1910
1420
1040
1190
1250
F factor usedF factors for Coal, Oil, and Gas
Anthrocite 2
Lignite
Natural
Propane
Butane
COAL
OIL
GAS
Bituminous 2
Fd Fw Fc
scf/MMBtu scf/MMBtu scf/MMBtu
O2
CO2
lbs/MMBtu
Page 1
Summary
Division of Air Quality
Reference Methods 5 - TSP
Compliance Demonstration of
Kennecott - SME005
Testing Results Lab Data - grams collected
Test Date 10/25/2023 10/25/2023 10/25/2023 10/25/2023 Lab Data Probe Filter Back
Circular Run 1 Run 2 Run 3 Run 4 Run 1 0.0038 0.0017 0.0079
As ft^2 1.67 1.67 1.67 Run 2 0.0045 0.005 0.002
Pbar 26.88 26.88 26.88 Run 3 0.0022 0.002 0.0019
Pq (static)0.46 0.46 0.46 Run 4
Ps 26.91 26.91 26.91
Avg. Ts F 164.46 163.92 165.88 Front Half Emissions Summary
CO2 - FCO2 0.10 0.10 0.10 Run 1 Run 2 Run 3 Run 4 Avg.
O2 20.60 20.60 20.60 gr./dscf 0.0023 0.0036 0.0015 0.0025
N2+C 79.30 79.30 79.30 lbs/hr 0.0356 0.0605 0.0268 0.0410
Md 28.84 28.84 28.84 lbs/MMBtu #VALUE!#VALUE!#VALUE!
Ms 28.62 28.63 28.65
Y 1.05 1.05 1.05
Cp 0.84 0.84 0.84 Total Emissions Summary w/back half condensable
Vm cf 39.08 43.05 44.28 Run 1 Run 2 Run 3 Run 4 Avg.
Vlc 16.20 16.70 15.70 gr./dscf 0.0056 0.0044 0.0022 0.0041
AVG. Tm F 71.02 72.00 65.44 lbs/hr 0.0868 0.0732 0.0389 0.0663
Vm std 36.75 40.44 42.13 lbs/MMBtu #VALUE!#VALUE!#VALUE!
Vw std 0.76 0.79 0.74
Bws 0.02 0.02 0.02
S Bws 0.40 0.39 0.41
Avg. Sqrt Dlp 0.37 0.40 0.42
Vs 24.09 26.02 27.15 F factor used
scfm wet 1836.12 1984.91 2064.83
acfm 2414.11 2607.47 2720.97
Qsd dscfh 107927.98 116824.12 121754.22
# Sample
Points 24.00 24.00 24.00
Dn 0.310 0.310 0.310
An 5.24E-04 5.24E-04 5.24E-04
Start Time 0:00 0:00 0:00
End Time 0:00 0:00 0:00
Total Test
time 60.00 60.00 60.00
Time @ point 2.50 2.50 2.50
80.00
90.00
100.00
110.00
120.00
1 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43 45 47
%
I
s
o
k
i
n
e
t
i
c
Points
Run 1 PxP Isokinetic
80.00
90.00
100.00
110.00
120.00
1 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43 45 47
%
I
s
o
k
i
n
e
t
i
c
Sample Points
Run 2 PxP Isokinetic
80.00
90.00
100.00
110.00
120.00
1 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43 45 47
%
I
s
o
k
i
n
e
t
i
c
Sample Points
Run 3 PxP Isokinetic
O2
CO2
lbs/MMBtu
80.00
90.00
100.00
110.00
120.00
1 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43 45 47
Sample Points
Run 4 PxP Isokinetic
Page 1
Run 1
Kennecott - SME005 Flow & Moisture Test Date 10/25/2023
As ft^2 Pbar Pq (static) Ps Avg. Ts F CO2 - FCO2 O2 N2+C Md Ms
1.67 26.88 0.46 26.91 164 0.10 20.60 79.30 28.84 28.62
Y Cp Vm cf Vlc Avg. Tm F Vm std Vw std Bws S Bws 0.3990
1.0500 0.84 39.076 16.20 71.02 36.750 0.763 0.0203 0.3990 0.999
Avg. Sqrt
Dlp Vs scfm wet acfm Qsd dscfh
# Sample
Points Dn
Total Test
time (minutes)
Time @ point
(minutes)Avg. Dlh
0.373 24.09 1,836 2,414 1.08E+05 24 0.31 60 2.50 1.133333
TRUE
Point No.Meter (cf)dl "p"dl "h"ts F tm F (in)tm F (out)Imp. Liquid Collected
1 81.838 0.16 1.30 164 62 83 Wt. (Final)Wt. (Initial)lc
2 83.547 0.14 1.10 163 59 82 488.00 482.90 5.1
3 85.162 0.15 1.20 165 58 80 641.40 640.20 1.2
4 86.827 0.15 1.20 170 57 80 711.80 712.30 -0.5
5 88.498 0.14 1.10 161 58 78 960.00 949.60 10.4
6 90.147 0.16 1.30 160 60 78 0.0
7 91.871 0.15 1.20 167 62 79
8 93.551 0.14 1.10 158 62 79 Isokinetics 108.6
9 95.168 0.12 1.00 165 62 80 Test Date 10/25/2023
10 96.684 0.13 1.00 164 61 81 Start Time enter
11 98.261 0.12 0.99 166 61 81 End Time
12 99.769 0.11 0.91 163 60 80 Run 1
13 101.217 0.16 1.30 162 61 81
14 103.112 0.15 1.20 166 60 81
15 104.804 0.16 1.30 167 61 82
16 106.551 0.14 1.10 169 61 82
17 108.172 0.15 1.20 169 60 82
18 109.843 0.14 1.20 158 61 83
19 111.501 0.13 1.10 163 61 83
20 113.057 0.14 1.20 167 61 83
21 114.710 0.13 1.10 167 61 84
22 116.285 0.13 1.10 164 62 84
23 117.858 0.12 1.00 164 62 84
24 119.381 0.12 1.00 165 62 84
25 120.914
26
27
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30
31
32
33
34
35
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Page 1
Run 2
Kennecott - SME005 Flow & Moisture Test Date 10/25/2023
As ft^2 Pbar Pq (static) Ps Avg. Ts F CO2 - FCO2 O2 N2+C Md Ms
1.67 26.88 0.46 26.91 164 0.10 20.60 79.30 28.84 28.63
Y Cp Vm cf Vlc Avg. Tm F Vm std Vw std Bws S Bws 0.3939
1.0500 0.84 43.053 16.70 72 40.442 0.786 0.0191 0.3939 0.999
Avg. Sqrt
Dlp Vs scfm wet acfm Qsd dscfh
# Sample
Points Dn
Total Test
time (minutes)
Time @ point
(minutes)Avg. Dlh
0.403 26.02 1,985 2,607 1.17E+05 24 0.31 60 2.50 1.37
TRUE
Point No.Meter (cf)dl "p"dl "h"ts F tm F (in)tm F (out)Imp. Liquid Collected
1 121.201 0.14 1.20 162.0 65.0 84.0 Wt. (Final)Wt. (Initial)lc
2 122.834 0.16 1.30 165.0 63.0 82.0 503.70 498.70 5.0
3 124.612 0.18 1.50 168.0 62.0 80.0 633.80 631.90 1.9
4 126.441 0.20 1.70 164.0 64.0 80.0 746.60 746.30 0.3
5 128.412 0.19 1.60 166.0 65.0 80.0 963.50 954.00 9.5
6 130.351 0.18 1.50 159.0 65.0 81.0 0.0
7 132.204 0.18 1.50 162.0 66.0 82.0
8 134.071 0.17 1.40 165.0 66.0 81.0 Isokinetics 110.4
9 135.861 0.17 1.40 163.0 66.0 80.0 Test Date 10/25/2023
10 137.671 0.18 1.50 167.0 64.0 79.0 Start Time
11 139.534 0.20 1.70 165.0 64.0 79.0 End Time
12 141.473 0.17 1.40 159.0 64.0 78.0 Run 2
13 143.287 0.17 1.40 162.0 63.0 78.0
14 145.521 0.18 1.50 166.0 62.0 79.0
15 147.412 0.16 1.40 159.0 62.0 80.0
16 149.178 0.17 1.40 163.0 62.0 81.0
17 151.007 0.15 1.30 165.0 61.0 79.0
18 152.724 0.14 1.20 163.0 61.0 80.0
19 154.412 0.16 1.40 160.0 61.0 80.0
20 156.172 0.15 1.30 167.0 61.0 80.0
21 157.881 0.14 1.20 165.0 62.0 82.0
22 159.547 0.12 1.00 166.0 62.0 84.0
23 161.102 0.13 1.10 168.0 64.0 84.0
24 162.712 0.12 1.00 165.0 65.0 83.0
25 164.254
26
27
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Page 1
Run 3
Kennecott - SME005 Flow & Moisture Test Date 10/25/2023
As ft^2 Pbar Pq (static) Ps Avg. Ts F CO2 - FCO2 O2 N2+C Md Ms
1.67 26.88 0.46 26.91 166 0.10 20.60 79.30 28.84 28.65
Y Cp Vm cf Vlc Avg. Tm F Vm std Vw std Bws S Bws 0.4124
1.0500 0.84 44.283 15.70 65 42.126 0.739 0.0172 0.4124 0.999
Avg. Sqrt
Dlp Vs scfm wet acfm Qsd dscfh
# Sample
Points Dn
Total Test
time (minutes)
Time @ point
(minutes)Avg. Dlh
0.420 27.15 2,065 2,721 1.22E+05 24 0.31 60 2.50 1.45
TRUE
Point No.Meter (cf)dl "p"dl "h"ts F tm F (in)tm F (out)Imp. Liquid Collected
1 164.558 0.15 1.20 162.0 65.0 75.0 Wt. (Final)Wt. (Initial)lc
2 166.214 0.17 1.40 170.0 55.0 75.0 488.8 482.5 6.3
3 168.114 0.20 1.60 168.0 54.0 76.0 640.8 640.6 0.2
4 170.094 0.15 1.20 168.0 53.0 74.0 712.0 711.8 0.2
5 171.782 0.22 1.80 172.0 52.0 73.0 969.0 960.0 9.0
6 173.812 0.18 1.50 153.0 52.0 72.0 0.0
7 175.671 0.15 1.30 153.0 52.0 73.0
8 177.358 0.19 1.60 152.0 52.0 74.0 Isokinetics 110.3
9 179.284 0.24 2.00 152.0 53.0 75.0 Test Date 10/25/2023
10 181.461 0.17 1.40 155.0 53.0 75.0 Start Time
11 183.267 0.14 1.20 151.0 53.0 76.0 End Time
12 184.904 0.16 1.30 160.0 54.0 77.0 Run 3
13 186.674 0.18 1.50 163.0 53.0 77.0
14 188.541 0.17 1.40 173.0 55.0 80.0
15 190.324 0.21 1.70 170.0 55.0 79.0
16 192.324 0.16 1.30 165.0 55.0 77.0
17 194.102 0.19 1.50 172.0 55.0 77.0
18 196.054 0.22 1.80 173.0 56.0 78.0
19 198.120 0.18 1.50 174.0 57.0 78.0
20 199.965 0.15 1.20 174.0 57.0 79.0
21 201.657 0.17 1.40 175.0 58.0 78.0
22 203.472 0.20 1.60 175.0 55.0 77.0
23 205.437 0.16 1.30 175.0 55.0 76.0
24 207.192 0.14 1.10 176.0 55.0 76.0
25 208.841
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Page 1