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HomeMy WebLinkAboutDRC-2023-001411 - 0901a068811869farll;� 1;;1,:;NERGYFUELS February 6, 2023 Sent VIA EXPEDITED DELIVERY Mr. Doug Hansen Director Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West Salt Lake City, UT 84116 an r /!' t I Energy Fuels Resource (USA) Inc. 225 Union Bhd. Suite 600 Lal,,rnood, CO, US, 80228 303 974 2140 ,1,111 .1.'11 ·r1:0_ t'ucbxom Re: Transmittal of 4th Quarter 2022 Groundwater Monitoring Report Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr. Hansen: Enclosed are two copies of the White Mesa Uranium Mill Groundwater Monitoring Report for the 4th Quarter of 2022 as required by the Groundwater Quality Discharge Permit UGW370004, as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours very truly iUU(Jt� E ERGV F ELS RESOURCES (USA) I C.Kathy Weinel Director, Regulatory Compliance cc: David Frydenlund Scott Bakken Logan Shumway Garrin Palmer Jordan App DRC-2023-001411 ?2e£rrJ --r ~ 1 r if ENERGY FUELS February 6, 2023 Sent VIA EXPEDITED DELIVERY Mr. Doug Hansen Director Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West Salt Lake City, UT 84116 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 ww,, .ener ,, ruels.com Re: Transmittal of 4th Quarter 2022 Groundwater Monitoring Report Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr. Hansen: Enclosed are two copies of the White Mesa Uranium Mill Groundwater Monitoring Report for the 4th Quarter of 2022 as required by the Groundwater Quality Discharge Permit UGW370004, as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours very truly itttu;Jt~ E ERGY F ELS RESO RCES (USA) I C. Kathy Weinel Director, Regulatory Compliance cc: David Frydenlund Scott Bakken Logan Shumway Garrin Palmer Jordan App White Mesa Uranium Mill Groundwater Monitoring Report State of Utah Groundwater Discharge Permit No. UGW370004 4th Quarter (October through December) 2022 Prepared by: ?'i:t;~ l:i'T:~ERGYFUELS Energy Fuels Resources (USA) Inc. 225 Union Boulevard, Suite 600 Lakewood, CO 80228 February 6, 2023 TABLE OF CONTENTS 1.0 INTRODUCTION ................................................................................................................ 1 2.0 GROUNDWATER MONITORING .................................................................................... 1 2.1 Samples and Measurements Taken During the Quarter .................................................... l 2.1.1 Groundwater Compliance Monitoring ....................................................................... I 2.1.2 Accelerated Groundwater Monitoring ....................................................................... 1 2.1.3 Background Well Monitoring .................................................................................... 2 2.1.4 TW4-24 ...................................................................................................................... 2 2.1.5 Parameters Analyzed ................................................................................................. 2 2.1.6 Groundwater Head Monitoring .................................................................................. 3 2.2 Field Data .......................................................................................................................... 3 2.3 Laboratory Results -Quarterly Sampling ......................................................................... 3 2.3.1 Copy of Laboratory Results ....................................................................................... 3 2.3.2 Regulatory Framework and Groundwater Background ............................................ .4 2.4 Laboratory Results -Accelerated Monitoring ................................................................. .4 2.4.1 Copy of Laboratory Results ...................................................................................... .4 2.4.2 Regulatory Framework and Groundwater Background ............................................ .4 2.4.3 Compliance Status ..................................................................................................... 5 2.5 Depth to Groundwater and Water Table Contour Map ..................................................... 5 3.0 QUALITY ASSURANCE AND DATA VALIDATION .................................................... 5 3 .1 Field QC Samples ............................................................................................................. 6 3.2 Adherence to Mill Sampling SOPs ................................................................................... 6 3 .3 Analyte Completeness Review ......................................................................................... 7 3 .4 Data Validation ................................................................................................................. 7 3.4.1 Field Data QA/QC Evaluation ................................................................................... 7 3.4.2 Holding Time Evaluation .......................................................................................... 9 3.4.3 Receipt Temperature Evaluation ............................................................................... 9 3.4.4 Analytical Method Checklist ..................................................................................... 9 3.4.5 Reporting Limit Evaluation ....................................................................................... 9 3 .4.6 Trip Blank Evaluation .............................................................................................. 10 3.4.7 QA/QC Evaluation for Routine Sample Duplicates ................................................ 10 3 .4.8 Radiologies Counting Error and Duplicate Evaluation ........................................... 11 3.4.9 Other Laboratory QA/QC ........................................................................................ 11 4.0 CORRECTIVE ACTION REPORT ................................................................................... 13 4.1 5.0 6.0 7.0 Assessment of Corrective Actions from Previous Period ............................................... 13 TIME CONCENTRATION PLOTS .................................................................................. 13 ELECTRONIC DATA FILES AND FORMAT ................................................................ 14 SIGNATURE AND CERTIFICATION ............................................................................. 15 Table 1 Table 2 Table 3 LIST OF TABLES Summary of Well Sampling for the Period Exceedances and Acceleration Requirements GWCL Exceedances INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports -Quarterly Sampling Tab F Laboratory Analytical Reports -Accelerated Monitoring Tab G Quality Assurance and Data Validation Tables G-lA/B G-2A/B G-3A/B G-4A/B G-5A/B G-6A/B G-7A/B G-8A/B G-9AIB Field Data QA/QC Evaluation Holding Time Evaluation Laboratory Receipt Temperature Check Analytical Method Check Reporting Limit Evaluation Trip Blank Evaluation QA/QC Evaluation for Sample Duplicates Radiologies Counting Error Laboratory Matrix QC Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter 11 coc CTF DWMRC EFRI GEL GWCLs GWDP LCS MS MSD QA QAP QC RPD SOPs USEPA ACRONYM LIST Chain-of-Custody Chemtech-Ford Utah Division of Waste Management and Radiation Control Energy Fuels Resources (USA) Inc. GEL Laboratories, Inc. Groundwater Compliance Limits Groundwater Discharge Permit Laboratory Control Spike Matrix Spike Matrix Spike Duplicate Quality Assurance Quality Assurance Plan Quality Control Relative Percent Difference Standard Operating Procedures United States Environmental Protection Agency 111 1.0 INTRODUCTION This is the Routine Groundwater Monitoring Report, as required under Part I.F .1 of State of Utah Groundwater Discharge Permit No. UGW370004 (the "GWDP") for the fourth quarter of 2022 for Energy Fuels Resources (USA) Inc. 's. ("EFRI's") White Mesa Uranium Mill (the "Mill"). As required under Parts I.E.1, I.E.2, I.E.3, and I.E.5 of the GWDP, this Report includes recorded field measurements and laboratory analyses for well monitoring conducted during the quarter. 2.0 GROUNDWATER MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of groundwater monitoring wells, piezometers, ex1stmg wells, chloroform contaminant investigation wells and nitrate contaminant investigation wells is attached under Tab A. Groundwater samples and measurements were taken during this reporting period, as discussed in the remainder of this section. 2.1.1 Groundwater Compliance Monitoring Groundwater samples and field measurements collected during the quarter included quarterly, semi-annual and accelerated monitoring. Accelerated monitoring is discussed below in Section 2.1.2. In this report, samples classified as being collected quarterly include those wells which are routinely sampled every quarter and the wells sampled semi-annually. Wells which are sampled routinely every quarter and semi-annually were analyzed for the parameters listed in Table 2 and Part I.E.1.d) 2)ii of the GWDP. Table 1 of this report provides an overview of wells sampled during the current period, along with the required sampling frequency applicable to each well during the current monitoring period, the date samples were collected from each well, and the date(s) analytical data were received from the contract laboratory(ies). Table 1 also indicates which sample numbers are associated with the required duplicates. During this quarter, three wells were resampled. MW-02, MW-32 and MW-39 were resampled for Gross Alpha minus radon and uranium ("gross alpha") because of laboratory issues. MW-26 and MW-39 were resampled on November 1, 2022 and MW- 32 was resampled on October 31, 2022. 2.1.2 Accelerated Groundwater Monitoring Accelerated monthly sampling was also performed ( quarterly wells accelerated to monthly), and results reported, for the wells indicated in Table 1. The accelerated sampling frequency, analyte list and well list were determined based on the previous analytical results as shown in Table 2. 1 Table 1 provides an overview of the wells sampled for the accelerated monthly program along with the routine sampling frequency as well as the accelerated sampling frequency, the date samples were collected from each well, the associated duplicates and the date(s) which analytical data were received from the contract laboratory(ies). 2.1.3 Background Well Monitoring Monitor wells MW-38, MW-39, and MW-40 were installed in the first quarter 2018 pursuant to the GWDP Part 1.H.2 and quarterly sampling commenced in fourth quarter 2018. The GWDP Part 1.H.3 requires the completion of a background report for each of these wells after the completion of 8 quarters of sampling. The background reports and resultant Groundwater Compliance Limits ("GWCLs") were calculated based on eight statistically valid data points. The background report for wells MW-38, MW-39 and MW-40 was submitted to DWMRC on March 4, 2021. EFRI submitted errata pages by letter dated June 7, 2021 based on the DWMRC review comments. The Background Report for MW-38, MW-39 and MW-40 was approved by DWMRC by letter dated June 16, 2021. MW-38, MW-39 and MW-40 will continue to be sampled on a quarterly basis until such time as these wells are included in the GWDP. The analytical results for MW-38, MW-39, and MW-40 for this period are included in TabE. 2.1.4 TW4-24 Pursuant to the GWDP, Part 1.E. l.c).ii, semi-annual monitoring of TW4-24 commenced in the second quarter of 2018. TW4-24 is currently used as a pumping well for the nitrate corrective action, is located within the chloroform plume, and is expected to exceed groundwater quality standards for analytes associated with these projects. It is expected that monitoring results will be highly variable as a result of the pumping and should not be used for direct compliance purposes. Rising or decreasing trends in analytes caused solely by pumping should not be unexpected. Further, as background cannot be established for this pumping well, and given the variability of background concentrations across the site, analyte concentrations in TW4-24 may also vary widely from site ranges due to natural background variability and/or localized changes resulting from long-term pumpmg. 2.1.5 Parameters Analyzed Routine quarterly groundwater monitoring samples were analyzed for the parameters listed in Table 2 and Part I.E. l.d) 2) ii of the GWDP. The accelerated monitoring samples were analyzed for a more limited and specific parameter list as shown in Table 2. 2 2.1.6 Groundwater Head Monitoring Depth to groundwater was measured in the following wells and/or piezometers, pursuant to Part I.E.3 of the GWDP: • The quarterly groundwater compliance monitoring wells (including MW-33 and MW-34). • Existing monitoring well MW-4 and the temporary chloroform investigation wells. • Piezometers -P-1, P-2, P-3A, P-4 and P-5. • Nitrate monitoring wells. • The DR piezometers which were installed during the Southwest Hydrogeologic Investigation. • In addition to the above, depth to water measurements are routinely observed m conjunction with sampling events for wells sampled during quarterly and accelerated efforts, regardless of the sampling purpose. Water levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab D. 2.2 Field Data Attached under Tab B are copies of field data sheets recorded in association with the quarterly effort for the groundwater compliance monitoring wells referred to in paragraph 2.1.1, above. Sampling dates are listed in Table 1. Attached under Tab C are copies of the field data sheets recorded in association with the accelerated monthly monitoring sampling efforts, referred to in paragraph 2.1.2, above. Sampling dates are listed in Table 1. 2.3 Laboratory Results -Quarterly Sampling 2.3.1 Copy of Laboratory Results Analytical results are provided by two contract analytical laboratories: GEL and Chemtech-Ford ("CTF"). Table 1 lists the dates when analytical results were reported to the Director, Regulatory Compliance for each well. 3 Results from analysis of samples collected under the GWDP (i.e., regular quarterly and accelerated samples) are provided in Tab E. Also included under Tab E are the results of analyses for duplicate samples as identified in Table 1. 2.3.2 Regulatory Framework and Groundwater Background Under the GWDP, background groundwater quality has been determined on a well-by- well basis, as defined by the statistics contained in the Decision Tree/Flowchart used for the previous Background Reports that was conditionally approved by the DWMRC on August 24, 2007. GWCLs that reflect this background groundwater quality have been set for compliance monitoring wells. Exceedances of the GWCLs during the preceding quarter determined the accelerated monthly monitoring program implemented during this quarter as noted in Tables 1 and 2. Exceedances of the GWCLs for this quarter are listed in Table 2 for sampling required under the revised GWDP. Accelerated requirements resulting from this quarter are highlighted for ease of reference. Table 3 documents the accelerated sampling program and shows the results and frequency of the accelerated sampling conducted. It should be noted, however, that, because the GWCLs have been set at the mean plus second standard deviation, or the equivalent, un-impacted groundwater would normally be expected to exceed the GWCLs approximately 2.5% of the time. Therefore, exceedances are expected in approximately 2.5% of sample results, and do not necessarily represent impacts to groundwater from Mill operations. In fact, more frequent sampling of a given analyte will increase the number of exceedances due to statistical variation and not due to Mill activity. Additionally, given the slow velocity of groundwater movement, accelerated sampling monthly may result in resampling of the same water and may lead to repeat exceedances for accelerated constituents not due to Mill activities, but due to repeat sampling of the same water. 2.4 Laboratory Results -Accelerated Monitoring 2.4.1 Copy of Laboratory Results Results from analysis of samples collected for the monthly accelerated sampling (i.e. quarterly accelerated to monthly) are provided in Tab F. Also included under Tab Fare the results of analyses for duplicate samples for this sampling effort, as identified in Table 1. 2.4.2 Regulatory Framework and Groundwater Background As a result of the issuance of a revised GWDP on March 8, 2021, which sets revised GWCLs, requirements to perform accelerated monitoring under Part LG.I of the previous GWDP ceased, effective March 8, 2021, and the effect of the issuance of the revised GWDP was to create a "clean slate" for most constituents going forward. 4 This means that accelerated monitoring during this quarter was required under the revised GWDP for only those constituents that exceeded the GWCLs since March 8, 2021. 2.4.3 Compliance Status Analytes that have exceeded the GWCLs set forth in the GWDP are summarized in Table 2. The analytes which exceeded their respective GWCLs during the quarter will be sampled on an accelerated schedule as noted in Table 2. A review of the accelerated data collected during the quarter is reported in EFRI's Exceedance Notice for the quarter. Part I.G.4 c) of the GWDP states, with respect to exceedances of GWCLs, "The Permittee shall prepare and submit within 30 calendar days to the Executive Secretary a plan and a time schedule for assessment of the sources, extent and potential dispersion of the contamination, and an evaluation of potential remedial action to restore and maintain groundwater quality to insure that Permit limits will not be exceeded at the compliance monitoring point and that DMT or BAT will be reestablished." EFRI submits an Exceedance Notice quarterly and the summary in the Exceedance Notice includes, for each exceedance, a brief discussion of whether such a plan and schedule is required at this time in light of other actions currently being undertaken by EFRI. The determination of whether a Plan and Time Schedule is required is based on discussions with DWMRC Staff in teleconferences on April 27 and May 2, 2011 and the constituents covered by previously submitted Source Assessment Reports. 2.5 Depth to Groundwater and Water Table Contour Map As stated above, a listing of groundwater level readings for the quarter ( shown as depth to groundwater in feet) is included under Tab D. The data from Tab D has been interpreted (kriged) and plotted in a water table contour map, provided under Tab H. The water table contour map provides the location and identity of the wells and piezometers for which depth to groundwater is recorded. The groundwater elevation at each well and piezometer, measured in feet above mean sea level, and isocontour lines to delineate groundwater flow directions observed during the quarter's sampling event are displayed on the map. 3.0 QUALITY ASSURANCE AND DATA VALIDATION The Mill Director, Regulatory Compliance performed a Quality Assurance/Quality Control ("QA/QC") review to confirm compliance of the monitoring program with requirements of the Groundwater Monitoring Quality Assurance Plan ("QAP"). As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and quality control review of laboratory data methods and data. Identification of field QC samples collected and analyzed is provided in Section 3 .1. Discussion of adherence to Mill sampling Standard Operating Procedures ("SOPs") is provided in Section 3.2. Analytical 5 completeness review results are provided in Section 3.3. The steps and tests applied to check laboratory data QA/QC are discussed in Sections 3.4.4 through 3.4.9 below. The Analytical Laboratories have provided summary reports of the analytical QA/QC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference certification and reporting protocol. The analytical laboratory QA/QC Summary Reports, including copies of the Mill's COC and Analytical Request Record forms for each set of Analytical Results, follow the analytical results under Tabs E and F. Review of the laboratory QA/QC information is provided under Tab G. 3.1 Field QC Samples The following field QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program: Two duplicate samples were collected during quarterly sampling as indicated in Table 1. The QC samples were sent blind to the analytical laboratory and analyzed for the same parameters as permit-required samples. One duplicate sample was collected during each month of accelerated sampling as indicated in Table 1. The QC samples were sent blind to the analytical laboratory and analyzed for the same accelerated parameters as the parent sample. Three trip blanks were provided by CTF and returned and analyzed with the quarterly monitoring samples. One trip blank for each of the monthly accelerated sample events was provided by CTF and returned and analyzed with the accelerated monthly monitoring samples. Rinsate samples were not collected during the quarter because equipment used during sample collection was dedicated and did not require decontamination. All wells except MW-20, MW-24, MW-37 and MW-38 have dedicated pumps for purging and sampling and as such no rinsate blanks samples are required. MW-20, MW-24, MW-37 and MW- 38 were purged and sampled with a disposable bailer and no rinsate blank was required. A deionized field blank was not required because equipment decontamination was not required and deionized water was not used during this sampling event. 3.2 Adherence to Mill Sampling SOPs On a review of adherence by Mill personnel to the existing sampling SOPs, the Director, Regulatory Compliance observed that QA/QC requirements established in the QAP were met and that the SOP's were implemented as required. 6 3.3 Analyte Completeness Review Analyses required by the GWDP for the quarterly and accelerated wells were performed. The accelerated sampling for the quarterly wells (quarterly to monthly) was completed as required by the GWDP and as shown in Tables 2 and 3. The monthly accelerated sampling program shown on Tables 2 and 3 is required as a result of exceedances in quarterly well monitoring results reported in previous quarters. 3.4 Data Validation The QAP and GWDP identify the data validation steps and data quality control checks required for the groundwater monitoring program. Consistent with these requirements, the Director, Regulatory Compliance completed the following evaluations: a field data QA/QC evaluation, a receipt temperature check, a holding time check, an analytical method check, a reporting limit check, a trip blank check, a QA/QC evaluation of routine sample duplicates, a QA/QC evaluation of accelerated sample duplicates, a gross alpha counting error evaluation and a review of each laboratory's reported QA/QC information. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab G. 3.4.1 Field Data QA/QC Evaluation The Director, Regulatory Compliance performs a review of field recorded parameters to assess their adherence with QAP requirements. The assessment involved review of two sources of information: the Field Data Sheets and the Quarterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and the stability of the following field parameters (based upon the purging method chosen): specific conductance, pH, temperature, redox potential, dissolved oxygen ["DO"] and turbidity. Stability of field parameters and well sampling techniques are dependent on the purging technique employed. Review of the Depth to Water data confirms that depth measurements were conducted within a five-day period. The results of this quarter's review are provided in Tab G. There are three purging strategies specified in the QAP that are used to remove stagnant water from the casing during groundwater sampling at the Mill. The three strategies are as follows: 1. Purging three well casing volumes with a single measurement of field parameters 2. Purging two casing volumes with stable field parameters (within 10% [Relative Percent Difference] ("RPD")) 3. Purging a well to dryness and stability ( within 10% RPD) of a limited list of field parameters after recovery During both the quarterly sampling event and the two monthly events, the purging technique used was two casing volumes with stable field parameters (pH, Conductivity, 7 Redox, temperature, DO, and turbidity) except for the following wells that were purged to dryness after 2 casing volumes were removed: MW-03A, MW-23, MW-24, and MW- 24A. Based upon the review of the Field Data Sheets, quarterly and semi-annually sampled locations conformed to the QAP requirement for purging using the two casing volume technique except for MW-20, MW-37 and MW-38. MW-20, MW-37 and MW-38 were evacuated to dryness before two casing volumes could be removed. MW-20, MW-37 and MW-38 have insufficient water to purge using a pump. Due to the small volume of water present, these wells are purged and sampled using a disposable bailer. MW-20, MW-37 and MW-38 conformed to the QAP, requirement for sampling low yield wells which includes the collection of three field parameters (pH, specific conductance ["conductivity"] and temperature) immediately prior to and immediately following sample collection. Stabilization of pH, conductivity and temperature were within the 10% RPD required by QAP. MW-03A, MW-23, MW-24, and MW-24A were purged to dryness after 2 casing volumes were removed and the low yield sampling procedures were used for the collection of field parameters. Stabilization of pH, conductivity and temperature were within the 10% RPD required by QAP for well MW-03A, MW-23, MW-24 and MW-24A. Additionally, two casing volumes were not purged from MW-26 and TW4-24, prior to sampling because MW-26 and TW4-24 are continuously pumped wells. If a well is continuously pumped, it is pumped on a set schedule per the remediation plan and is considered sufficiently evacuated to immediately collect a sample; however, if a pumping well has been out of service for 48 hours or more, EFRI follows the purging requirements outlined in Attachment 2-3 of the QAP. The review of the field sheets for compliance with QAP requirements resulted in the observations noted below. The QAP requirements in Attachment 2-3 specifically state that field parameters must be stabilized to within 10% over at least two consecutive measurements. The QAP Attachment 2-3 states that turbidity should be less than 5 NTU prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP Attachment 2-3 does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements greater than 5 NTU below are included for information purposes only. • Turbidity measurements were less than 5 NTU for the quarterly and semi-annual wells except MW-5, MW-17, MW-25, MW-27, MW-29, MW-31, MW-32, and MW-32 Resample. Per the QAP, Attachment 2-3, turbidity measurements prior to sampling were within a 10% RPD for the quarterly and semi-annual wells. • Turbidity measurements were less than 5 NTU for the accelerated sampling wells except MW-11 and MW-31 in the November monthly event. As previously noted, the QAP does not require that turbidity be less than 5 NTU. Turbidity measurements prior to sampling were within a 10% RPD for the accelerated sampling wells 8 The other field parameters ( conductance, pH, red ox potential, DO and temperature) for the wells were within the required RPD for the quarterly, semi-annual and accelerated sampling. During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water for the quarterly, semi-annual and accelerated sampling programs to the nearest 0.01 foot. EFRI's letter to DWMRC of March 26, 2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In response to DWMRC's subsequent correspondence dated June 1, 2010 and June 24, 2010, EFRI has completed a monitoring well redevelopment program. The redevelopment report was submitted to DWMRC on September 30, 2011. DWMRC responded to the redevelopment report via letter on November 15, 2012. Per the DWMRC letter dated November 15, 2012, the field data generated this quarter is compliant with the turbidity requirements of the approved QAP. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided under Tab G. The samples were received and analyzed within the required holding time. 3.4.3 Receipt Temperature Evaluation COC sheets were reviewed to confirm compliance with the QAP requirement in Table 1 that samples be received at 6°C or lower. Sample receipt temperature checks are provided under Tab G. The quarterly, semi-annual and accelerated samples were received within the required temperature limit. As noted in Tab G, samples for gross alpha analyses were shipped without using ice. Per Table 1 in the approved QAP, samples submitted for gross alpha analyses do not have a sample temperature requirement. 3.4.4 Analytical Method Checklist The analytical methods reported by both laboratories were checked against the required methods specified in the QAP. Analytical method check results are provided in Tab G. The review indicated that the quarterly, semi-annual and accelerated samples were analyzed in accordance with Table 1 of the QAP. 3.4.5 Reporting Limit Evaluation The analytical method RLs reported by both laboratories were checked against the RLs specified in the QAP Table 1. RL evaluations are provided in Tab G. The analytes were 9 measured and reported to the required RLs except that several sets of quarterly, semi- annual and accelerated sample results had the RL raised for at least one analyte due to matrix interference and/or sample dilution as noted in Section 3.4.9. In all cases the reported value for the analyte was higher than the increased RL. 3.4.6 Trip Blank Evaluation The trip blank results were reviewed to identify any VOC sample contamination which is the result of sample handling and shipment. Trip blank evaluations are provided in Tab G. The trip blank results associated with the quarterly, semi-annual and accelerated samples were all nondetect for VOCs. 3.4.7 QA/QC Evaluation for Routine Sample Duplicates Section 9.1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples .. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results are less than 5 times the detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for the duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits; however, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPO is greater than 20%. The additional duplicate information is provided for information purposes. Field duplicate sample results were assessed as required by the SOP. Duplicate results were within the acceptance limits specified in the QAP except for fluoride and manganese in MW-35/MW-70. The fluoride results were greater than 20% RPD, however, the sample and duplicate results were not greater than 5 times the RL and as such are acceptable. The manganese results were greater than 20% RPO, and the sample and duplicate results were greater than 5 times the RL. The approved QAP specifies a separate corrective action for duplicate RPDs outside of acceptance limits. The revised procedure for duplicate results outside of acceptance limits was implemented for the results outside of the acceptance limits. The corrective actions that were taken in accordance with the QAP procedure are as follows: the Director, Regulatory Compliance contacted the Analytical Laboratory and requested a review of the raw data to assure that there were no transcription errors and the data were accurately reported. The laboratory noted that the data were accurate and reported correctly. Reanalysis was not completed. Field duplicate results are shown in Attachment G. The duplicate results were within a 20% RPD in the monthly accelerated samples. Results of the RPD test are provided under Tab G. 3.4.8 Radiologies Counting Error and Duplicate Evaluation Section 9.14 of the QAP requires that when gross alpha results are reported with an activity equal to or greater than the GWCL the counting variance shall be equal to or less than 20% of the reported activity concentration. An error term may be greater than 20% of the reported activity concentration when the sum of the activity concentration and error term is less than or equal to the GWCL. The quarterly and semi-annual radiologic sample results met the counting error requirements specified in the QAP except as noted in Tab G. The results for MW-02 Resample, MW-26, MW-31, MW-32 Resample, MW- 36, and MW-40 did not meet the requirement that the counting error be equal to or less than 20% of the reported activity concentration, likely because the reported concentrations are very near the RL. As stated above the error term may be greater than 20% of the reported activity concentration when the sum of the activity concentration and error term is less than or equal to the GWCL. The results for MW-02 Resample, MW-26, MW-31, MW-32 Resample, and MW-36, passed the secondary check; however, MW-40 does not have a GWCL and this second level check cannot be performed. The results are usable for the intended purpose and there is no adverse effect on the data. Section 9.4 of the QAP also requires a comparability check between the sample and field duplicate sample results utilizing the formula provided in the text. All of the radiologic duplicates were within acceptance limits. Results of quarterly, semi-annual, and accelerated radiologic sample QC are provided under Tab G. 3.4.9 Other Laboratory QA/QC Section 9.2 of the QAP requires that the laboratory's QNQC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate analytical laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, EFRI's Director, Regulatory Compliance rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided under Tab G. The lab QNQC results from both GEL and A WAL samples for compounds regulated under the GWDP met these requirements. The check samples included at least the following: a method blank, a laboratory control spike ("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the equivalent, where applicable. It should be noted that: • Laboratory fortified blanks are equivalent to LCSs. • Laboratory reagent blanks are equivalent to method blanks. • Post digestion spikes are equivalent to MSs. 11 • Post digestion spike duplicates are equivalent to MSDs. • Laboratory Duplicates are equivalent to MSDs. The qualifiers, and the corresponding explanations reported in the QA/QC Summary Reports for the check samples for the analytical methods were reviewed by the Director, Regulatory Compliance. The QAP, Section 8.1.2 states that an MS/MSD pair may be analyzed with each analytical batch depending on the analytical method specifications. The QAP does not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the MS/MSD pair be prepared on EFRI samples only. Acceptance limits for MS/MSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the specifications in the analytical methods to analyze either an MS or MS/MSD pair with each analytical batch were met as applicable to each method. While the QAP does not require it, the recoveries were reviewed for compliance with the laboratory established acceptance limits. The QAP does not require this level of review and the results of this review are provided for information only. The information from the Laboratory QNQC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for the quarterly and semi-annual samples were within acceptable laboratory limits for the regulated compounds except as indicated in Tab G. The data recoveries and RPDs which are outside the laboratory established acceptance limits do not affect the quality or usability of the data because the recoveries and RPDs above or below the acceptance limits are indicative of matrix interference most likely caused by other constituents in the samples. Matrix interferences are applicable to the individual sample results only. The specifications in the analytical methods to analyze a MS/MSD pair with each analytical batch (as applicable to the methods) was met and as such the data are compliant with the QAP. The information from the Laboratory QNQC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for the accelerated samples were within acceptable laboratory limits for the regulated compounds except as indicated in Tab G. The data recoveries and RPDs which are outside the laboratory established acceptance limits do not affect the quality or usability of the data because the recoveries and RPDs above or below the acceptance limits are indicative of matrix interference most likely caused by other constituents in the samples. Matrix interferences are applicable to the individual sample results only. The specifications in the analytical methods to analyze a MS/MSD pair with each analytical batch (as applicable to the methods) was met and as such the data are compliant with the QAP. The QAP specifies that surrogate compounds shall be employed for all organic analyses but the QAP does not specify acceptance limits for surrogate recoveries. The information from the Laboratory QNQC Summary Reports indicates that the surrogate recoveries for the quarterly and accelerated samples were within acceptable laboratory limits for the surrogate compounds. 12 The information from the Laboratory QA/QC Summary Reports indicates that the LCS recoveries for both the quarterly and accelerated samples were within acceptable laboratory limits except for sulfate in the accelerated monthly samples. The low sulfate LCS recovery is indicative of a low bias to the sample results; however the result was only slightly below the acceptance limit and likely do not affect the usability of the data. Further, sulfate is ubiquitous in groundwater and the analytical results this quarter fall within the historic ranges for samples at the Mill. The QAP, Section 8.1.2 requires that each analytical batch shall be accompanied by a method blank. The analytical batches routinely contain a blank, which is a blank sample made and carried through all analytical steps. For the Mill samples, a method blank was prepared for the analytical methods. Per the approved QAP, contamination detected in analysis of method blanks will be used to evaluate any analytical laboratory contamination of environmental samples. The QAP states that non-conformance conditions will exist when contaminant levels in the samples(s) are not an order of magnitude greater than the blank result. All method blanks for both the quarterly and accelerated samples were nondetect. Method blank results are included in Tab E and Tab F. Laboratory duplicates are completed by the analytical laboratories as required by the analytical method specifications. Acceptance limits for laboratory duplicates are set by the laboratories. The QAP does not require the completion of laboratory duplicates or the completion of a QA assessment of them. EFRI reviews the QC data provided by the laboratories for completeness and to assess the overall quality of the data provided. Duplicate results for the quarterly, semi-annual and accelerated samples outside of the laboratory established acceptance limits are included in Tab G. The results outside of the laboratory established acceptance limits do not affect the quality or usability of the data because the RPDs above the acceptance limits are indicative of non-homogeneity in the sample matrix. Matrix affects are applicable to the individual sample results only. 4.0 CORRECTIVE ACTION REPORT There are no corrective actions required during the current monitoring period. 4.1 Assessment of Corrective Actions from Previous Period No corrective actions were identified in the previous report. 5.0 TIME CONCENTRATION PLOTS Time concentration plots for each monitoring well for the following constituents: chloride, fluoride, sulfate, and uranium, are included under Tab I. The data points collected to date are reflected on the plots. 13 Time concentration plots included with quarterly groundwater reports prior to and including first quarter 2012 did not include data that were determined to be outliers using the statistical methods used for the background determinations at the Mill. Based on conversations with DWMRC, all of the data have been included in the quarterly time concentration plots since first quarter 2012. 6.0 ELECTRONIC DATA FILES AND FORMAT EFRI has provided to the Director electronic copies of the laboratory results from groundwater quality monitoring conducted during the quarter in Comma Separated Values format, from the analytical laboratories. A copy of the transmittal e-mail is included under Tab J. 14 7.0 SIGNATURE AND CERTIFICATION This document was prepared by Energy Fuels Resources (USA) Inc. Energy Fuels Resources (USA) Inc. By: Scott A. Bakken Vice President, Regulatory Affairs 15 Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Scott A. Bakken Vice President, Regulatory Affairs Energy Fuels Resources (USA) Inc. 16 Tables Table 1: Summary of Well Sampling for the Quarter Normal Purpose for sampling this Well Frequency quarter Sample Date Date of Lah Report MW-01 Semi-annually General Monitoring Well 10/19/22 (11/10/22) [11/22/22] MW-02 Semi-annually Semi-annually 10/20/22 (11/10/22) MW-02 Resample Semi-annually Semi-annually 11/01/22 [12/6/22) MW-03A Semi-annually Semi-annually 10/19/22 (11/10/22) [11/22/22] MW-05 Semi-annually Semi-annually 10/12/22 (11/1/22) [11/15/22] MW-11 Quarterly Quarterly 10/10/22 (11/1/22) [11/15/22] MW-12 Semi-annually Semi-annually 10/13/22 (11/1/22) [11/15/22] MW-14 Quarterly Quarterly 10/11/22 (11/1/22) [11/15/22] MW-15 Semi-annually Semi-annually 10/12/22 (11/1/22) [11/15/22] MW-17 Semi-annually Semi-annually 10/17/22 (11/10/22) [ 11/22/22] MW-18 Semi-annually General Monitoring Well 10/18/22 (11/10/22) [ 11/22/22] MW-19 Semi-annually General Monitoring Well 10/17/22 (11/10/22) [11/22/22] MW-20 Semi-annually General Monitoring Well 11/01/22 (l 1/29/22)(12/21/22) [12/6/22) MW-22 Semi-annually General Monitoring Well 10/19/22 (11/10/22) [11/22/22] MW-23 Semi-annually Semi-annually 11/01/22 (11/29/22) ( 12/21122) [12/6/22] MW-24 Semi-annually Semi-annually 11/02/22 (11/29/22) (12/21122) [12/6/22] MW-24A Semi-annually Semi-annually 11/02/22 (11/29/22) (12121/22) [12/6/22] MW-25 Quarterly Quarterly 10/10/22 (11/1/22) [11/15/22] MW-26 Quarterly Quarterly 10/13/22 (11/1/22) [11/15/22] MW-27 Semi-annually Semi-annually 10/19/22 (11/10/22) [11/22/22) MW-28 Semi-annually Semi-annually 10/12/22 (11/1/22) [11/15/22] MW-29 Semi-annually Semi-annually 10/12/22 (11/1/22) [11/15/22] MW-30 Quarterly Quarterly 10/13/22 (11/1/22) [11/15/22] MW-31 Quarterly Quarterly 10/11/22 (11/1/22) [11/15/22] MW-32 Semi-annually Semi-annually 10/11/22 (11/1/22) MW-32 Resample Semi-annually Semi-annually 10/31/22 [12/6/22] MW-35 Semi-annually Semi-annually 10/31/22 (11/29/22)(12/21/22) [12/6/22] MW-36 Quarterly Quarterly 10/11/22 (11/1/22) [11/15/22] MW-37 Semi-annually Semi-annually 11/01/22 (11/29/22) (12121122) [12/6/22] MW-38 Background Background 11/01/22 (11/29/22)(12/21/22) [12/6/22] MW-39 Background Background 10/20/22 (11/10/22) MW-39 Resample Background Background 11/01/22 [12/6/22] MW-40 Background Background 10/18/22 (11/10/22) [11/22/22] TW4-24 Semi-annually General Monitoring Well 11/01/22 (11/29/22)(12121/22) [12/6/22] MW-65 1 per Batch Duplicate ofMW-12 10/13/22 (11/1/22) [11/15/22] MW-70 1 per Batch Duplicate ofMW-35 10/31/22 (11/29/22) (12/21122) [12/6/22] Accelerated November Monthly MW-11 Monthly Accelerated 11/08/22 12/2/2022 MW-25 Monthly Accelerated 11/09/22 12/2/2022 MW-26 Monthly Accelerated 11/10/22 12/2/2022 MW-30 Monthly Accelerated 11/09/22 12/2/2022 MW-31 Monthly Accelerated 11/08/22 12/2/2022 MW-65 1 per Batch Duplicate ofMW-30 11/09/22 12/2/2022 Accelerated December Monthly MW-11 Monthly Accelerated 12/14/22 01/03/23 MW-25 Monthly Accelerated 12/14/22 01/03/23 MW-26 Monthly Accelerated 12/15/22 01/03/23 MW-30 Monthly Accelerated 12/13/22 01/03/23 MW-31 Monthly Accelerated 12/13/22 01/03/23 MW-65 1 per Batch Duplicate ofMW-30 12/13/22 01/03/23 Notes: Multiple dates shown for a single laboratory depict resubmission dates for the data. Resubmissions were required to correct reporting errors. When multiple dates are shown for a single laboratory, the final submission date is shown in italics. Dates in parenthesis depicts the date that data was reported by Chemtech-Ford (CTF). Dates in brackets are the date and data reported by GEL laboratories. Table 2 Exceedances and Acceleration Requirements Monitoring Well GWCLin First Result Routine Sample Accelerated Exceedance Start of Accelerated Constituent Exceeding GWCL Current Exceeding the (Water Class) GWDP GWCL Frequency Frequency Sample Period Monitoring Quarterly Wells Accelerated to Monthly Sampling MW-11 (Class II) Total Dissolved Solids (mg/L) 2528 2680 Quarterly Monthly Q3 2021 November 2021 Manganese (ug/L) 237 376 Quarterly Monthly Q3 2021 November 2021 Nitrate+ Nitrite (as N) (mg/L) 2.5 2.55 Quarterly Monthly Ql 2022 June 2022 Chloride (mg/L) 39.16 48.4 Quarterly Monthly Q3 2019 Q4 2019 (November) Selenium (ug/L) 12.5 15.5 Quarterly Monthly Q4 2022 March 2023 Sulfate (mg/L) 1309 14IO Quarterly Monthly Q3 2019 Q4 2019 (November) MW-25 (Class III) Chloride (mg/L) 35 35.8 Quarterly Monthly Q42022 March 2023 Total Dissolved Solids (mg/L) 2976 3100 Quarterly Monthly Q3 2021 November 2021 MW-26 (Class III) Nitrate+ Nitrite (as N) (mg/L) 0.62 1.3 Quarterly Monthly QI 20IO May 20IO Chloroform (ug/L) 70 700 Quarterly Monthly Ql 2010 May2010 Total Dissolved Solids (mg/L) 3284.19 3390 Quarterly Monthly Q3 2021 November 2021 Chloride (mg/L) 58.31 72 Quarterly Monthly QI 20IO May2010 Carbon Tetrachloride ( ug/L) 5 26.1 Quarterly Monthly QI 2021 Q2 2021 Methylene Chloride (ug/L) 5 6.59 Quarterly Monthly Q3 2020 August 2020 MW-30 (Class II) Nitrate + Nitrite (as N) (mg/L) 2.5 16.1 Quarterly Monthly QI 2010 May2010 Chloride (mg/L) 128 134 Quarterly Monthly QI 2011 May2011 Total Dissolved Solids (mg/L) 1918 20IO Quarterly Monthly Q3 2021 November 2021 Field pH (S.U.) 6.47 6.37 Quarterly Monthly Q4 2022 March 2023 Selenium (ug/L) 53.6 56.3 Quarterly Monthly QI 2021 Q2 2021 Uranium (ug/L) 9.82 10.2 Quarterly Monthly Ql 2021 Q2 2021 MW-31 (Class III) Nitrate+ Nitrite {as N) {mg/L) 5 21.7 Quarterly Monthly QI 2010 May2010 Total Dissolved Solids (mg/L) 2132 2580 Quanerly Monthly Q3 2019 Q4 2019 (November) Uranium {ug/L) 15 15.5 Quarterly Monthly Q22020 August 2020 Sulfate (mg/L) 993 1150 Quarterly Monthly QJ 2019 Q4 2019 (November) Chloride (mg/L) 143 145 Quarterly Monthly Ql 2011 Mo.y2011 Semi-Annual Wells Accelerated to Quarterly Sampling Monitoring Well GWCLin First Result Sample Accelerated Exceedance Start of Accelerated Constituent Exceeding GWCL Current Exceeding the (Water Class) GWDP GWCL Frequency Frequency Sample Period Monitoring MW-12 (Class III) Uranium (ug/L) 23.5 23.7 Semi-Annually Quarterly Q2 2017 Q3 2017 Selenium (ug/L) 39 41.2 Semi-Annually Quarterly Q2 2020 Q3 2020 MW-17 (Class Ill) Chloride (mg/L) 46.8 54.0 Semi-Annually Quarterly Q42022 Q2 2023 MW-24 (Class Ill) Cadmium (ug/L) 6.43 6.97 Semi-Annually Quarterly Q22018 Q3 2018 (September) Beryllium (ug/L) 2 2.42 Semi-Annually Quarterly Q4 2017 QI 2018 Thallium (u_g/L) 2.01 2.44 Semi-Annually Quarterly Q2 2018 Q3 2018 (September) Nickel (ug/L) 50 57.7 Semi-Annually Quarterly Q42018 Q3 2019 Sulfate (mg/L) 2903 2960 Semi-Annually Quarterly Ql 2020 Q3 2020 Manganese (ug/L) 7507 7700 Semi-Annually Quarterly Q4 2019 QI 2020 Fluoride (mg/L) 0.47 0.797 Semi-Annually Quarterly Q4 2018 Q3 2019 Gross Alpha (pCi/L) 7.5 9.03 Semi-Annually Quarterly Q4 2020 Q3 2021 TDS(mg/L) 4450 4460 Semi-Annually Quarterly Q2 2021 Q3 2021 Field pH (S.U.) 5.03 4.45 Semi-Annually Quarterly Q2 2018 Q3 2018 (September) MW-27 (Class III) Nitrate+ Nitrite (as N) (mg/L) 5.6 5.8 Semi-Annually Quarterly Q2 2010 Q3 2010 Fluoride (mg/L) 0.85 0.90 Semi-Annually Quarterly Q2 2022 Q3 2022 MW-28 (Class Ill) Chloride (mg/L) 105 108 Semi-Annually Quarterly Q2 2010 Q3 2010 Nitrate+ Nitrite (as N) (mg/L) 5 5.14 Semi-Annually Quarterly Q4 2019 Q3 2020 Selenium (u_g/L) 11. l 12.4 Semi-Annually Quarterly Q2 2019 Q3 2019 Cadmium (ug/L) 5.2 5.41 Semi-Annually Quarterly Q2 2014 Q4 2014 Uranium (ug/L) 4.9 61.3 Semi-Annually Quarterly Q2 2014 Q4 2014 MW-29 (Class III) Uranium (ug/L) 15 15.3 Semi-Annually Quarterly Q42020 Q3 2021 MW-32 (Class Ill) Chloride (mg/L) 35.99 36.3 Semi-Annually Quarterly Q2 2014 (QI Q2 2014 2015) MW-37 (Class Ill) Field pH (S.U.) 6.61 6.60 Semi-Annually Quarterly Q42022 Q2 2023 Notes: Highlighted text shows accelerated requirements resulting from Q4 2022 sampling event. Monitoring Well (Water Constituent Exceeding GWCL Class) Nitrate + Nitrite (as N) (mg/L) Chloride (mg/L) MW-11 Manganese (ug/L) (Class II) Sulfate (mg/L) TDS (mg/L) Selenium (ug/L) MW-25 (Class TDS (mg/L) lll) Chloride (mg/L) Nitrate+ Nitrite (as N) (m2/L) MW-26 Chloroform (ug/L) (Class ill) Chloride (mv/1 ) Nitrate+ Nitrite (as N) (m_g/L) Chloride (mfllL) MW-30 Selenium (u_g/L) (Class II) Field pH (S.U.) Uranium (ug/L) Nitrate+ Nitrite (ns N) (mg/L) Sulfate (mg/L) MW-31 TDS (mg/L) (Class III) Uranium (ug/L) Chloride (m_g/L) MW-12 Uranium (uw'L) (Class lll) Selenium (ug/L) MW-17 Chloride (mg/L) (Class III) Beryllium (ug/L) Cadmium (u_g/L) Fluoride (mg/1 ) Nickel (ml!/L) MW-24 Manaanese (u2/L) (Class III) Thallium (ug/L) Gross Alpha (oCi/L) Sulfate (mg/L) TDS (mg/L) Field pH (S.U.) MW-27 Nitrate+ Nitrite (as N) (mg/L) (Class III) Fluoride (mg/L) Chloride (mg/L) MW-28 Selenium (ug/L) (Class III) Nitrate+ Nitrite (as N) (ml!/L) Uranium (ug/L) MW-29 Uranium (ug/L) (Class Ill) MW-32 Chloride (mg/L) (Class LU) MW-37 Field pH (S.U.) (Class III) Notes: NS= Not Required and Not Sampled NA= Not Applicable Exceedances are shown in yellow GWCLin QI 2021 March 8, 2021 Sample Date GWDP 2.5 39.16 237 1/12/21 1309 2528 12.5 2976 1/11/21 35 0.62 70 1/14/21 58.3 1 2.5 128 53.6 1/11/21 6.47 -8.5 9.82 5 993 2132 1/12/21 15 143 23.5 39 1/14/21 46.8 NS 2 6.43 0.47 50 7507 2.01 1/14/21 7.5 2903 4450 5.03 -8.5 5.6 1/14/21 0.85 105 11.1 1/15/21 5 4.9 15 1/15/21 35.39 1/14/21 6.61 -8.5 NS QI 2021 Results February February March March 2021 2021 Ql 2021 2021 2021 Result Monthly Monthly Monthly Monthly Sample Sample Date Result Date Result Required Quarterly Sampling Wells 1.21 NA NA 46.4 46.4 46.9 185 254 221 2/9/21 3/8/21 1140 1260 1270 2010 2160 1950 <5 NA NA 2660 NS NA NS NA 34 NA NA 0.619 0.764 0.617 2200 2/10/21 1930 3/9/21 2190 57.4 71.3 63.9 17.7 14.3 17.0 184 189 192 55.6 2/10/21 55.3 3/9/21 56.3 7.49 7.25 7.14 9.86 11.6 10.2 17.J 14.3 17.4 1070 1130 1210 2460 2/9/21 2960 3/8/21 2400 19.7 22.2 20.2 354 380 388 Required Semiannual Sampling Wells 25.0 35.1 NS NA NS NA NA NS NA NS NA 2.75 NA NA 8.79 NA NA 0.916 NA NA 70.4 NA NA 7460 NA NA 2.74 NS NA NS NA 2.94 NA NA 2980 NA NA 4260 NA NA 5.08 NA NA 5.1 6 NS NA NS NA NA 128 NA NA 14.0 NS NA NS NA 3.44 NA NA 10.3 NA NA 16.9 NS NA NS NA 36.9 NS NA NS NA NA NS NA NS NA iThese GWCLs were reset with the issuance of the March 8, 2021 GWDP. iThe new GWCLs became effective on March 8, 2021 and the first exceedance under the revised GWDP was noted in the March monthly data. -., Table 3 GWCL Exceedances under the March 8 2021 GWDP Q2 2021 Results May2021 June2021 Q2 2021 May 2021 June 2021 Q3 2021 Q22021 Monthly Monthly Sample Result Sample Monthly Sample Monthly Sample Date Result Result Date Date Date Required Quarterly Sampling Wells 0.948 NA NA 47.7 46.4 52.1 237 NA NA 04/20/21 5/10/21 6/8/21 7/27/21 1290 1280 1270 2110 2190 1960 <5 NA NA 04/14/21 2720 NA NA NS NS 7/28/21 34.8 NA NA 1.42 1.06 0.368 04/21/21 777 5/11/21 733 6/8/21 1590 7/28/21 57.5 69.6 54.9 17.7 18.6 17.0 162 188 170 04/14/2 I 55.7 5/11/21 58.3 6/8/21 54.1 7/29/21 7.20 7.20 7.36 10.3 10.7 9.84 18.6 18.9 20.6 1170 1200 1170 04/13/21 2300 5/10/21 2610 6/7/21 2400 7/27/21 20.1 21.7 20.8 377 384 374 Required Semiannual Sampling Wells 22.9 4/20/21 28.8 NS NA NS NA 7/21/21 4/26/21 32.6 NS NA NS NA NS 2.78 NA NA 8.08 NA NA 0.925 NA NA 72.4 NA NA 7540 NA NA 4/29/21 3.02 NS NA NS NA 7/29/21 3.18 NA NA 2960 NA NA 4460 NA NA 5.00 NA NA 6.57 4/15/21 NS NA NS NA 7/22/21 0.69 144 NA NA 4/15/21 13.4 NS NA NS NA 7/23/21 4.09 NA NA 8.52 NA NA 4/14/21 16.2 NS NA NS NA 7/22/2 I 4/13/21 31.8 NS NA NS NA 7/28/2 I 5/12/21 7.00 NS NA NS NA NS Q3 2021 Results Q4 2021 Results August August September September November 2021 Q4 2021 November December December Q3 2021 2021 2021 2021 Q4 2021 2021 2021 2021 2021 Result Monthly Monthly Monthly Monthly Sample Result Monthly Monthly Monthly Monthly Sample Date Date Result Sample Date Result Sample Date Result Sample Date Result Required Quarterly Sampling Wells Required Quarterly Sampling Wells 0.924 NA NA 1.5 NA NA 48.3 57.0 49.6 52.8 53.6 53.9 376 NA NA 8/10/21 9/7/21 10/20/21 286 11/16/21 261 12/13/21 300 1470 1370 1240 1360 1300 1350 2680 NA NA 2200 2230 2140 <5 NA NA 6.75 NA NA 3100 NA NA 2680 2920 2590 NS NS 10/20/21 11/16/21 12/14/2 1 34.2 NA NA 33.1 NA NA 0.352 1.42 0.710 0.928 1.18 1.76 723 8/10/21 996 9/9/21 516 10/21/21 540 11/16/21 568 12/15/21 1160 54.0 61.4 59.3 55.2 56.9 75.9 20.6 16.5 15.4 14.3 18.0 18.6 188 161 183 182 182 184 56.3 8/9/2 I 56.J 9/8/21 60.4 10/19/21 54.6 11/17/21 53.6 12/14/21 58.8 6.98 6.84 6.70 6.77 7.18 7.04 9.60 9.38 9.74 9.76 9.67 JO.I 18.7 15.7 16.0 18.1 19.3 17.9 1210 1130 1130 1220 1180 1220 3100 8/9/21 2600 9/7/21 2870 10/19/21 2600 11/15/21 2610 12/13/21 2420 20.0 19.3 20.2 20.9 21.5 21.8 391 365 356 371 366 376 Required Semiannual Sampling Wells Required Semiannual Sampling Wells 22.2 32.4 NS NA NS NA 11/9/21 23.1 26.4 NS NA NS NA NA NS NA NS NA 11/8/21 33.4 NS NA NS NA 2.71 NA NA 2.66 NA NA 9.26 NA NA 9.30 NA NA 1.4 NA NA 0.988 NA NA 76.7 NA NA 76.7 NA NA 7890 NA NA 7430 NA NA 2.91 NS NA NS NA 11/10/21 3.14 NS NA NS NA 1.92 NA NA 1.56 NA NA 3050 NA NA 3220 NA NA 4940 NA NA 4730 NA NA 5.85 NA NA 5.23 NA NA 6.32 3.88 NS NA NS NA 10/26/21 NS NA NS NA NA 0.65 152 NA NA 147 NA NA 18.5 NS NA NS NA 10/26/21 11.2 NS NA NS NA 6.09 NA NA 1.89 NA NA 13.80 NA NA 6.03 NA NA 15.8 NS NA NS NA 10/27/21 14,9 NS NA NS NA 36.5 NS NA NS NA 11/2/21 36.1 NS NA NS NA NA NS NA NS NA 11/17/21 7.06 NS NA NS NA Monitoring Well (Water Class) MW-11 (Class II) MW-25 (Class III) MW-26 (Class III) MW-30 (Class II) MW-31 (Class III) MW-12 (Class III) MW-17 (Class III) MW-24 (Class III) MW-27 (Class III) MW-28 (Class III) MW-29 (Class III) MW-32 (Class rm MW-37 (Clas.s III) Ql 2022 Results February February March2022 March GWCLin Ql 2022 Ql 2022 2022 2022 Monthly 2022 Constituent Exceeding GWCL March 8, 2021 Sample Result Monthly Monthly Sample Monthly GWDP Date Sample Result Date Result Date Required Quarterly Sampling Wells Nitrate+ Nitrite (as N) (mg/L) 2.5 2.55 NA NA Chloride (mg/L) 39.16 51.1 57.2 67.7 Manganese (ug/1..) 237 156 233 224 1/18/22 2/8/22 3/8/22 Sulfate (mg/I..) 1309 1020 1240 1170 TDS (mg/L) 2528 2050 1900 2080 Selenium {ug/L) 12.5 9.29 NA NA TDS (mg/I..) 2976 1/17/22 2720 2/9/22 2690 3/7/22 2610 Chloride (mg/L) 35 34.1 NA NA Nitrate+ Nitrite (as N) (mwl.) 0.62 0.601 0.367 0.600 Chloroform (ug/L) 70 1/20/22 818 2/9/22 1580 3/8/22 1460 Chloride (m.!!IL) 58.31 77.1 58.6 64.J Nitrate+ Nitrite (as N) (mg/L) 2.5 14.5 13.6 16.6 Chloride (mg/L) 128 181 184 196 Selenium (ug/L) 53.6 1/17/22 56.7 2/9/22 57.7 3/7/22 62.0 Field pH (S.U.) 6.47 -8.5 7.62 7.20 7.12 Uranium (ug/L) 9.82 JO.I 10.3 9.9 Nitrate+ Nitrice (as N) (mg/L) 5 18.0 13.5 17.0 Sulfate (mg/L) 993 1210 1250 731 TDS (rnwl.) 2132 1/19/22 2620 2/8/22 2680 3/7/22 2530 Uranium (u2/L) 15 21.7 22.1 22.5 Chloride ( m.!!IL) 143 370 379 416 Required Semiannual Sampling Wells Uranium (ug/L) 23.5 22.1 1/20/22 NS NA NS NA Selenium (ug/L) 39 25.6 Chloride (mg/L) 46.8 NS NA NS NA NS NA Beryllium (ug/L) 2 2.71 NA NA Cadmium (ug/L) 6.43 8.46 NA NA Fluoride (mo-/1 ) 0.47 1 NA NA Nickel (m2/L) 50 80.9 NA NA MM.e.anese (uwL) 7507 7630 NA NA Thallium (u2/L) 2.01 1/27/22 2.66 NS NA NS NA Gross Aloha (oCi/L) 7.5 2.26 NA NA Sulfate (mg/L) 2903 3060 NA NA TDS (rng/L) 4450 4140 NA NA Field pH (S.U.) 5.03 -8.5 5.31 NA NA Nitrate+ Nitrite (as N) (mg/L) 5.6 6.25 1/18/22 NS NA NS NA Fluoride ( mg/L) 0.85 NA Chloride (mg/L) 105 140 NA NA Selenium (ug/L) 11.1 1/20/22 13.3 NS NA NS NA Nitrate+ Nitrite (as N) (mg/L) 5 4.03 NA NA Uranium (ug/L) 4.9 8.50 NA NA Uranium (ug/L) 15 1/18/22 JS.I NS NA NS NA Chloride (mg/L) 35.39 1/19/22 35.0 NS NA NS NA Field pH (S.U.) 6.61 -8.5 NS NA NS NA NS NA Pursuant to the DWMRC letter of August 8, 2022, these constituents w,11 no longer be monitored on an accelerated schedule. These constituents will be dropped from this report after this quarter. Table 3 -GWCL Exceedances under the March 8, 2021 GWDP Q2 2022 Results May2022 June2022 Q22022 Q2 2022 Monthly May2022 Monthly June2022 Q32022 Sample Result Sample Monthly Sample Monthly Sample Date Date Result Date Result Date Required Quarterly Sampling Wells 2.2 1.6 1.9 54.9 59.5 46.4 4/18/22 180 5/4/22 254 6/6/22 228 7/12/22 1240 1270 866 2060 2290 2360 10.8 NA NA 4/12/22 3600 5/3/22 2660 6/7/22 2730 7/13/22 33.4 NA NA 0.8 1.1 0.60 4/20/22 447 5/4/22 616 6/7/22 1250 7/14/22 56.8 63.2 47.4 17 15 11.0 173 195 126 4/20/22 64.9 5/4/22 69.4 6/7/22 65.7 7/13/22 6.92 7.24 7.32 9.6 JO.I 9.6 18.0 13.0 13.0 1180 1220 1110 4/11/22 4300 5/3/22 2660 6/6/22 2690 7/12/22 22.0 22.9 21.5 372 381 351 Required Semiannual Sampling Wells 4/19/22 20.5 31.3 NS NA NS NA 7/14/22 4/18/22 31.5 NS NA NS NA NS 2.5 NA NA 9.20 NA NA 0.8 NA NA 74.3 NA NA 7070 NA NA 7/20/22 4/27/22 3.1 NS NA NS NA 7/28/22 2.28 NA NA 3120 NA NA 3350 NA NA 4.81 NA NA 6.30 _4/12/22 NS NA NS NA 7/15/22 0.90 130 NA NA 4/19/22 19.8 NS NA NS NA 7/15/22 5.1 NA NA JO.IO NA NA 4/14/22 15.7 NS NA NS NA 7/14/22 4/11/22 28.6 NS NA NS NA 7/15/22 5/17/22 7.04 NS NA NS NA NS Q3 2022 Results Q4 2022 Results August August September September November November December December Q32022 2022 2022 2022 2022 Q42022 Q42022 2022 2022 2022 2022 Result Monthly Monthly Monthly Monthly Sample Result Monthly Monthly Monthly Monthly Sample Result Sample Date Result Date Sample Date Result Sample Date Result Date Required Quarterly Sampling Wells Required Quarterly Sampling Wells 2.12 2.45 2.65 2.90 2.74 1.30 54.0 67.4 68.1 72.1 71.9 52.3 297 8/8/22 201 212 9/21/22 10/10/22 214 11/8/22 220 273 12/14/22 1390 1260 1300 1140 1140 1330 2520 3230 2280 2570 2270 2370 9.3 NA NA 15.5 NA NA 2830 2780 2750 2660 2690 2780 8/9/22 9/20/22 10/10/22 11/9/22 12/14/22 22.4 NA NA 35.8 NA NA 1.63 1.56 0.491 0.632 0.408 2.66 <1.0 8/9/22 1120 9/20/22 810 10/13/22 749 11/10/22 512 12/15/22 460 61.0 65.0 62.1 65.5 59.2 60.6 17.6 13.5 16.5 17.9 15.9 16.1 108 185 182 196 156 195 61.1 8/9/22 64.3 9/20/22 70.0 10/13/22 65.1 11/9/22 75.6 12/13/22 70.8 7.33 7.33 6.81 6.84 6.37 6.59 10.0 JO.I 8.3 9.8 JO.I 13.0 16.9 16.8 17.1 17.0 16.0 12.6 1260 1230 1200 972 1380 1280 2700 8/8/22 2700 9/20/22 2830 10/11/22 2720 I 1/8/22 2670 12/13/22 2700 22.6 22.7 18.8 23.3 24.5 26.2 421 396 390 397 243 335 Required Semiannual Sampling Wells Required Semiannual Sampling Wells 21.6 29.2 NS NA NS NA 10/13/22 21.2 32.1 NS NA NS NA NA NS NA NS NA 10/17/22 54.0 NS NA NS NA 2.7 NA NA 3.3 NA NA 8.6 NA NA 10.9 NA NA 0.760 NA NA 1.53 NA NA 69.9 NA NA 86.9 NA NA 7540 NA NA 8130 NA NA 3.0 NS NA NS NA 11/2/22 3.5 NS NA NS NA 2.55 NA NA 2.70 NA NA 2800 NA NA 2680 NA NA 4200 NA NA 4440 NA NA 4.89 NA NA 4.39 NA NA 4.80 5.18 5.26 NS NA NS NA 10/19/22 NS NA NS NA 0.530 0.722 159 NA NA 161 NA NA 20.8 NS NA NS NA 10/12/22 23.7 NS NA NS NA 5.16 NA NA 5.69 NA NA 12.4 NA NA 12.5 NA NA 15.1 NS NA NS NA 10/12/22 15.2 NS NA NS NA 28.2 NS NA NS NA 10/11/22 37.1 NS NA NS NA NA NS NA NS NA 11/1/22 6.60 NS NA NS NA INDEX OFT ABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab Cl Field Data Worksheets Accelerated Monitoring, November 2022 Tab C2 Field Data Worksheets Accelerated Monitoring, December 2022 Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports -Quarterly Sampling Tab F Laboratory Analytical Reports -Accelerated Monitoring Tab Fl Laboratory Analytical Reports -Accelerated Monitoring, November 2022 Tab F2 Laboratory Analytical Reports -Accelerated Monitoring, December 2022 Tab G Quality Assurance and Data Validation Tables G-lA/B G-2A/B G-3A/B G-4A/B G-5A/B G-6A/B G-7A/B G-8 A/B G-9A/B Field Data QA/QC Evaluation Holding Time Evaluation Laboratory Temperature Check Analytical Method Check Reporting Limit Evaluation Trip Blank Evaluation QA/QC Evaluation for Sample Duplicates Radiologies Counting Error Laboratory Matrix QC Tab H Kriged Current Quarterly Groundwater Contour Map Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter Tab A Site Plan and Perched Well Locations White Mesa Site TW4-43 ~ TWN-20 D MW-24A • TW4-42 ¢ TW4-40 EB TW4-19 EB MW-38 -¢- MW-5 • TW4-12 0 TWN-7 ◊ PIEZ-1 " DR-14 DR-17 . DR-20 perched monitoring well installed July, 2022 temporary perched monitoring well installed September, 2021 temporary perched nitrate monitoring well installed April, 2021 perched monitoring well installed December 2019 temporary perched monitoring well installed April 2019 perched chloroform pumping well installed February 2018 perched chloroform or nitrate pumping well perched monitoring well installed February 2018 perched monitoring well temporary perched monitoring well temporary perched nitrate monitoring well perched piezometer RUIN SPRING o seep or spring l . "··'' \ DR-23 . • .. MW-29 . ' DR-10 DR-11 DR-12 DR-13 •· MW-JA • MW-21 ,. Ml -01 :,bandonod () lWN-05 • MW-18 :1b:,ndoncd () lWN-15 aba(ldoned () lWN-10 abandont'ld () lWN-11 () lWN-14 ,1/xmdfJned () lWN-09 () lWN-06 ,1bnridonod () lWN-08 PIEZ-01 • MW-19 CJ () () lWN-18 lWN-20 lWN-07 CeU 2 • MW-30 Cd!3 • MW-17 "'iwti03 PIEZ-02 <> I '11 -02• lWN-0~. Mt- 21i~11L.Sit_ e J" ~ ilk ,- ·--(> ... lWN-01,PIEZ,.JA \: 1W4-210 ,, ...., ,TW4-'18_ ~~U.~c.-:,,~~ ' TIii "Ui''m'""o.,.,-·-•p·: . -l41ll·.WW<P.1WA-2 ;.41'0Jt,'+JS~12 f,\W1~ TW-41i'll;,wii~ ,W.g(:oV"~ Mt~, TW4-1,;;:.:_;, i1~•·U 0 ~~~~.04 . ,lY/~7~~..:oi/iw..,,, ~jJ\. •. _-,w~i MW-U -0.,. ~""'1,, ~ · -~-. TWc-1, E ... ri· 4-2lhA/;1-31 C,11&_(;) .. 0 ~--~JW "!'il'il~ QTW•~o ~~ 1WJ'9"vfn'14-43 TWH~ tw'i~ 1W""2o 0 PIEZ-05 ◊ MW-40 abandon red () lWN-12 <> () lWN-16 abandone-d () lWN-17 TWN-19 DR-15 • DR-21 - I <( ◊ MW-39 u, • ·LU .. ◊ MW-20 ·:E MW-38 I liJ ~· ' ~--;:--. ~~--··-:~.,-=~~-:, • --- MW-22 .,.~ rtJ 1" mile HYDRO GEO CHEM, INC. WHITE MESA SITE PLAN SHOWING LOCATIONS OF PERCHED WELLS AND PIEZOMETERS APPROVED DATE REFERENCE H:/718000/nov22/Uwelloc0922.srf FIGURE A-1 TabB Field Data Worksheets Quarterly Sampling Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-01 Sampling Program Sampling Program Field Sample ID MW-01 10192022 Sampling Event Sampling Event 2022 Q4 GW Quarterly 2022 Q4 GW Quarterly Purge Date & Time 10/19/2022 7:10 Sample Date & Time 10/19/2022 10:10 I sampler [sampler I TH/DL TH/DL Purging Equipment Pump Weather Conditions Clear Pump Type QED External Ambient Temperature (C) 7 Purging Method 2 Casings Previous Well Sampled MW-03A Casing Volume (gal) 19.37 Calculated Casing Volumes Purge Duration (min) 178.52 pH Buffer 7.0 7.0 Well Depth (ft) 118.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 3 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 65.22 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/19/2022 10:07 38.40 1788 6.80 14.22 284 0 9.1 10/19/2022 10:08 38.62 1787 6.83 14.28 263 0 9.0 10/19/2022 10:09 38.84 1780 6.85 14.21 250 0 9.1 10/19/2022 10:10 39.06 1776 6.87 14.27 238 0 9.1 Pumping Rate Calculations \Volume of water purged (gals) 39.06 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 180.00 [Final Depth to Water (feet) 97.41 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory GEL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Gross Alpha y WATER 1 250-ml HDPE y HNO3 y Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HNO3 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 DegC y Comments: I Arrived on site at 0705. Purge began at 0710. Purged well for a total 180 minutes. Purge ended and samples collected at 1010. Water was clear, left site at 1020. Signature of Field Technician ~---'----~;-"'·~ ~~~~ f 0) I Groundwater Discharge Permit ~ .II ._. r ~/~v~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-02 Sampling Program Sampling Program Field Sample ID MW-02 10202022 Sampling Event Sampling Event 2022 Q4 GW Quarterly 2022 Q4 GW Quarterly Purge Date & Time 10/20/2022 7:10 Sample Date & Time 10/20/2022 9:10 !sampler [sampler I TH/DL TH/DL Purging Equipment Pump Weather Conditions Clear Pump Type QED External Ambient Temperature (C) 6 Purging Method 2 Casings Previous Well Sampled MW-39 Casing Volume (gal) 12.66 Calculated Casing Volumes Purge Duration (min) 116.75 pH Buffer 7.0 7.0 Well Depth (ft) 128.80 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 109.40 Conductivity Dissolved Date!Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/20/2022 9:07 25.38 3688 6.95 14.66 426 0 19.9 10/20/2022 9:08 25.60 3630 6.95 14.53 425 0 18.0 10/20/2022 9:09 25.82 3650 6.97 14.57 424 0 18.0 10/20/2022 9:10 26.04 3663 6.97 14.50 423 0 17.9 Pumping Rate Calculations [voll!fTle _of water purged (g!'s) 26.04 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 120.00 I Final Depth to Water (feet) 117.75 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: I Arrived on site at 0705. Purge began at 0710. Purged well for a total of 120 minutes. Purge ended and samples collected at 0910. Water was clear. Left site at 0920. Signature of Field Technician ~~,t,~ I Groundwater Discharge Permit ·,~ _ .,~YFVEZS Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-02 Sampling Program Field Sample ID MW-02 11012022 Sampling Event 2022 MW-02 and MW-39 Resample Purge Date & Time 11/1/2022 7:55 Sample Date & Time 11/1/2022 9:55 [sampler TH/DL Purging Equipment Pump Weather Conditions Clear Pump Type QED External Ambient Temperature (C) 3 Purging Method 2 Casings Previous Well Sampled MW-39 Casing Volume (gal) 12.68 Calculated Casing Volumes Purge Duration (min) 116.87 pH Buffer 7.0 7.0 Well Depth (ft) 128.80 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 109.38 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 11/1/2022 9:52 25.38 3759 6.78 13.89 400 0 33.4 11/1/2022 9:53 25.60 3768 6.80 13.76 398 0 32.5 11/1/2022 9:54 25.82 3762 6.85 13.86 397 0 32.1 11/1/2022 9:55 26.04 3750 6.87 13.89 395 0 32.1 Pumping Rate Calculations [volume of water purged (gals) 26.04 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 120.00 [Final Depth to Water (feet) 117.85 Number of casing Volumes 2.00 Volume, if well evacuated to dryness O 0 Name of Certified Analytical Laboratory_ GEL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number I Type Sample Filtered? Type I Added? Gross Alpha y WATER 1 I 250-ml HOPE y HN03 I y Comments: [ Arrived on site at 0752. Pur9~ began at 0755. Purged well for a total of 120 minutes. Purge ended and samples collected at 0955. Water was clear. Left site at 1000. Signature of Field Technician ~~-;' Groundwater Discharge Permit ~ -/ . r-,. '. -/ ~,...~ -~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-03a Sampling_ Program Field Sample ID MW-03A 10192022 Saml)lil'lg Event 2022 Q4 GW Quarterly_ Purge Date & Time 10/18/2022 12:15 Sample Date & Time 10/19/2022 8:00 [sampler Purging Equipment Pump Weather Conditions Pump Type QED External Ambient Temperature (C) Purging Method 2 Casings Previous Well Sampled Casing Volume (gal) 7.16 Calculated Casing Volumes Purge Duration (min) 68.87 pH Buffer 7.0 7.0 Well Depth (ft) pH Buffer 4.0 4.0 Well Casing Diameter (in) Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) Conductivity DatefTime Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) 10/18/2022 13:25 14.56 5791 6.84 17.70 411 0 10/19/2022 7:59 5805 6.53 14.87 10/19/2022 8:09 5820 6.57 14.80 Pumping Rate Calculations [volume of water purged (galsJ 14.56 Flow Rate (Q = S/60) (gal/min) Time to evacuate 2 Casing Volumes (min) [ Final Depth to Water (feet) 91.85 Number of casing Volumes Volume, if well evacuated to dryness (gals) Name of Certified Analytical Laboratory AWSL Analytical Sam_e_les Information Sample Container Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 DegC Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2) voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C Nutrients y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C General lnorganics y WATER 1 250-ml HDPE u 4 DegC Gross Alpha y WATER 1 250-ml HDPE y HNO3 Comments: Arrived on site at 1211. Purge began at 1215. Purged well for a total of 70 minutes. Purged well dry. Purge ended at 1325. Water was clear. Left site at 1327. Arrived on site at 0752. Depth to water was 86.93. Samples collected at 0800. Left site at 0811 . Signature of Field Technician 2)~#~ TH/DL Sunny 16 MW-40 95.00 4 84.03 Dissolved Oxygen(%) Before/After 79.0 Before After .208 70.00 2.00 14.56 Preservative Added? y y y y y y Groundwater Discharge Permit =--~ .. .,,.,.-~~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-OS Sampling Program Field Sample ID MW-OS 10122022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 10/12/2022 10:45 Sample Date & Time 10/12/2022 14:15 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 15 Purging Method 2 Casings Previous Well Sampled MW-28 Casing Volume (gal) 21.87 Calculated Casing Volumes Purge Duration (min) 201.61 pH Buffer 7.0 7.0 Well Depth (ft) 141.50 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 108.00 Conductivity Dissolved DatefTime Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/12/2022 14:12 44.91 2841 7.05 15.25 356 10.5 10.6 10/12/2022 14:13 45.13 2850 7.15 15.30 345 11.0 10.5 10/12/2022 14:14 45.35 2849 7.20 15.23 336 11.3 10.4 10/12/2022 14:15 45.57 2843 7.23 15.24 329 12.0 10.6 Pumping Rate Calculations [volume of water purge~_9_als) 45.57 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 [Final Depth to Water (feet) 126.30 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40mlVOA y HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: [ Arrived on site at 1042. Purge be_gan at 1045. Purged well for a total of 21 O minutes. Purge ended and samples collected at 1415. Left site at 1425. Signature of Field Technician ~~--rr~~~ Groundwater Discharge Permit F-:.~ v-.~ . ~ _--,,'/~Y~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-11 Sampling Program Field Sample ID MW-11 10102022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 10/10/2022 9:30 Sample Date & Time 10/10/2022 14:00 I sampler I TH/DL I Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 12 Purging Method 2 Casings Previous Well Sampled MW-25 Casing Volume (gal) 29.16 Calculated Casing Volumes Purge Duration (min) 268.84 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 85.33 Conductivity pH (pH Dissolved Date/Time Gallons Purged (gal) (umhos/cm) Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/10/2022 13:57 57.93 3031 6.97 16.40 395 0 9.4 10/10/2022 13:58 58.15 3050 7.00 16.14 392 0 9.5 10/10/2022 13:59 58.37 3044 7.05 16.00 391 0 9.5 10/10/2022 14:00 58.59 3063 7.07 15.98 389 0 9.6 !volume of water purged (gals) Pumping_ Rate Calculations 58.59 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 270.00 I Final Depth to Water (feet) 87.03 Number of casing Volumes 2.00 Volume, if well evacuated to dryness() 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/ Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 DegC y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: I Arrived on site at 0925. Purge began at 0930. Purged well for a total of 270 minutes. PurQe ended and samples collected at 1400. Water was clear. Left site at 1410. Signature of Field Technician --=3~-a~ --··~ •'~.::..ua~FVELS Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 10/13/2022 9:02 27.55 10/13/2022 9:03 27.77 10/13/2022 9:04 27.99 10/13/2022 9:05 28.21 jvolume of water purged Jg_als) [Final Depth to Water (feet) Name of Certified Analytical Laboratory AWSL Analy_tical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater ~---------------~-----------------------~ MW-12 Samelin_g Program MW-12 10132022 Sampling_ Event 2022 Q4 GW Quarterly 10/13/2022 6:55 10/13/2022 9:05 \sampler TH/DL Pump Weather Conditions Sunny QED External Ambient Temperature (C) 10 2 Casings Previous Well Sampled MW-30 13.68 126.08 7.0 Well Depth (ft) 130.40 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 109.45 Conductivity pH (pH Dissolved (umhos/cm) Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4194 6.52 13.60 320 0 22.1 4222 6.53 13.90 323 0 20.0 4254 6.55 13.87 325 0 20.0 4212 6.57 14.00 327 0 19.0 Pumping Rate Calculations 28.21 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 130.00 122.05 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HDPE u 4 DegC y y WATER 1 250-ml HOPE y HN03 (pH<2) y y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-ml HDPE u 4 Deg C y y WATER 1 250-ml HDPE y HN03 y [Arrived on site at 0650. Purge began at 0655. Pur.9ed well for a total of 130 minutes. Purge ended and samples collected at 0905. Water was clear. Left site at 0915. Signature of Field Technician ~~-r,rc-r~ Groundwater Discharge Permit ·•~··· 1·· ~ :a ,,-•,, ,=;,-=zs , .. ___ ,,··~/~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-14 Sampling Program Field Sample ID MW-14 10112022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 10/11/2022 12:00 Sample Date & Time 10/11/2022 14:50 !sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 20 Purging Method 2 Casings Previous Well Sampled MW-31 Casing Volume (gal) 17.76 Calculated Casing Volumes Purge Duration (min) 163.70 pH Buffer 7 .0 7.0 Well Depth (ft) 128.70 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 101.50 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 10/11/2022 14:47 36.23 3781 6.50 15.01 365 0 1.8 10/11/2022 14:48 36.45 3670 6.53 15.01 364 0 1.9 10/11/2022 14:49 36.67 3703 6.55 15.00 363 0 1.9 10/11/2022 14:50 36.89 3716 6.56 15.00 263 0 1.9 Pumping Rate Calculations ~olume of water purged (gals) 36.89 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 170.00 I Fin_al Depth to Water (feet) 101.82 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2504 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: [Arrived _on site at 1157. Purge began at 1200. Pur9ed well for a total of 170 minutes. Purge ended and samples collected at 1450. Water was clear. Left site at 1500. Signature of Field Technician .:3 t..,.<......- Groundwater Discharge Permit ~ . ------~-. ~ .--V EIVERJGY, Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-15 Sampling Program Field Sample ID MW-15 10122022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 10/12/2022 7:10 Sample Date & Time 10/12/2022 10:30 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 8 Purging Method 2 Casings Previous Well Sampled MW-29 Casing Volume (gal) 20.77 Calculated Casing Volumes Purge Duration (min) 191.50 pH Buffer 7.0 7.0 Well Depth {ft) 137.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 105.18 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 10/12/2022 10:27 42.74 4230 6.74 15.15 292 0 18.4 10/12/2022 10:28 42.96 4263 6.74 15.10 292 0 18.2 10/12/2022 10:29 43.18 4221 6.74 15.09 291 0 18.3 10/12/2022 10:30 43.40 4241 6.74 15.11 291 0 18.3 Pumping Rate Calculations [\/_olume of water purged (gals) 43.4 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 200.00 [ Final Depth to Water (feet) 107.81 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4DegC y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2} y voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2}, 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2}. 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HN03 y Comments: [ Arrived on site at 0705. Purge began at 0710. Purged well for a total of 200 minutes. Purge ended and samples collected at 1030. Water was clear. Left site at 1040. Signature of Field Technician ~<.<A.,._,_ Groundwater Discharge Permit ~ . -~-. -.• I-.,-~·· ' ___ .... l { / ~l ' 'I ,· t" ~.,,..~ . ~ -~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-17 Sampling Program Sampling Program Field Sample ID MW-17 10172022 Sampling Event Sampling Event 2022 Q4 GW Quarterly 2022 Q4 GW Quarterly Purge Date & Time 10/17/2022 7:00 Sample Date & Time 10/17/2022 11:00 !sampler [sampler I TH/DL TH/DL Purging Equipment Pump Weather Conditions Clear Pump Type QED External Ambient Temperature (C) 5 Purging Method 2 Casings Previous Well Sampled MW-19 Casing Volume (gal) 25.85 Calculated Casing Volumes Purge Duration (min) 238.00 pH Buffer 7.0 7.0 Well Depth (ft) 112.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 72.40 Conductivity pH (pH Dissolved Date/Time Gallons Purged (gal) (umhos/cm) Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 10/17/2022 10:57 51.42 3707 6.62 15.10 451 160.0 12.0 10/17/2022 10:58 51.64 3679 6.64 14.95 449 162.0 12.1 10/17/2022 10:59 51.86 3699 6.64 14.93 448 164.0 12.2 10/17/2022 11:00 52.08 3697 6.66 14.91 447 165.0 12.3 Pumping Rate Calculations !volume of water purged (gals) 52.08 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 240.00 I Final Depth to Water (feet) 86.78 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Anal~ical San,_eles Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-mL HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-mL HDPE y HNO3 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-mL HDPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-mL HDPE u 4 Deg C y Gross Alpha y WATER 1 250-mL HDPE y HNO3 y Comments: Arrived on site at 0655. Purge began at 0700. Purged well for a total of 240 minutes. Purge ended and samples collected at 1100. Water was clear but had tiny little bubbles surfacing. Left site at 1110. Signature of Field Technician ~~~/4~ I Groundwater Discharge Permit ~. I'·;·-,.,,,-• .-: J .EJl'laEiRIGY, . •' Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-18 Sampling Program Field Sample ID MW-18 10182022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 10/18/2022 6:45 Sample Date & Time 10/18/2022 12:45 !sampler I TH/DL I Purging Equipment Pump Weather Conditions Clear Pump Type QED External Ambient Temperature (C) 6 Purging Method 2 Casings Previous Well Sampled MW-17 Casing Volume (gal) 38.93 Calculated Casing Volumes Purge Duration (min) 358.80 pH Buffer 7.0 7.0 Well Depth (ft) 134.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 74.37 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 10/18/2022 12:42 77.46 3398 6.49 14.70 401 0 3.0 10/18/2022 12:43 77.68 3393 6.50 14.75 397 0 3.0 10/18/2022 12:44 77.90 3398 6.50 14.73 394 0 3.1 10/18/2022 12:45 78.12 3395 6.51 14.73 391 0 3.1 Pumping Rate Calculations [volume of water purged (gals) 78.12 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 360.00 [ Final Depth to_ V'.later (feet} 75.35 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Anal}'t_ical Laboratory AWSL Anal ytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HNO3 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HNO3 y Comments: [ Arrived on site at 0640. Purge began at 0645. Purged well for a total of 360 minutes. Purge ended and samples collected at 1245. Water was clear. Left site at 1255. Signature of Field Technician ~ ~ - 'FiP'S /•=-E7¥ERGY~ . , Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date!Time Gallons Purged (gal) 10/17/2022 14:22 107.84 10/17/2022 14:23 108.06 10/17/2022 14:24 108.28 10/17/2022 14:25 108.50 [volume of water purged (gals) [ Final Depth to Water (feet) Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-19 Sampling Program MW-19 10172022 Sampling_ Event 2022 Q4 GW Quarterly 10/17/2022 6:05 10/17/2022 14:25 [sampler TH/DL Pump Weather Conditions Clear QED External Ambient Temperature (C) 5 2 Casings Previous Well Sampled MW-20 53.64 494.41 7.0 Well Depth (ft) 149.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 66.85 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 1376 6.48 15.30 413 2.5 133.0 1373 6.50 15.30 412 2.6 132.0 1374 6.53 15.32 411 2.7 133.0 1370 6.57 14.30 411 2.6 133.0 Pumping Rate Calculations 108.50 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 500.00 77.89 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE u 4 Deg C y y WATER 1 250-ml HDPE y HN03 (pH<2) y y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-ml HDPE u 4 Deg C y y WATER 1 250-ml HDPE y HN03 y I Arrived on site at 0600. Purge b.E!gan at 0605. Purged well for a total of 500 minutes. Purg_e ended and samples collected at 1425. Water was clear. Left site at 1435. Signature of Field Technician ~~~ Groundwater Discharge Permit v;I:-,--,. r, '~y~ s ·. / Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-20 Sampling Program Sampling Program Field Sample ID MW-20 11012022 Sampling Event Sampling_ Event 2022 Q4 GW Quarterly 2022 Q4 GW Quarterly Purge Date & Time 10/14/2022 10:12 Sample Date & Time 11/1/2022 12:00 !sampler !sampler I TH/DL TH/DL Purging Equipment Bailer Weather Conditions Sunny Pump Type Grundfos External Ambient Temperature (C) 14 Purging Method 2 Casings Previous Well Sampled MW-37 Casing Volume (gal) 4.97 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 92.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 84.38 Conductivity Dissolved Date!Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/14/2022 10:15 5.00 6326 6.73 15.01 412 18.0 81.8 11/1/2022 12:00 5640 6.91 14.13 11/1/2022 12:03 5669 6.92 14.10 !Volume of water purged (gals) 7.50 Pumpin_g Rate Calculations Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () [Final Depth to Water (feet) 91.98 Number of casing Volumes Volume, if well evacuated to dryness (gals) Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Total Dissolved Soi Ids y WATER 1 250-ml HDPE u 4 DegC Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2) voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C Nutrients y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C General lnorganics y WATER 1 250-ml HOPE u 4 Deg C Gross Alpha y WATER 1 250-ml HDPE y HN03 Comments: Arrived on site at 1007. Bailing began at 1012. Bailed a total of 7.5 gallons from well. Bailed well dry. Bailing ended at 1022. Water was a little murky. Left site at 1024. Arrived on site at 1156. Depth to water was 89.35. Samples bailed and collected at 1200. Left site at 1205. Signature of Field Technician .:=)~/4~ Before After 1.50 7.50 Added? y y y y y y I Groundwater Discharge Permit ~ .I ,..-,...= ' .. .,· .. · ,•~y,_.__. ' !:I Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-22 Sampling Program Field Sample ID MW-22 10192022 Sampli11__g Event 2022 Q4 GW Quarterly Purge Date & Time 10/19/2022 8:20 Sample Date & Time 10/19/2022 13:20 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 7 Purging Method 2 Casings Previous Well Sampled MW-01 Casing Volume (gal) 31.05 Calculated Casing Volumes Purge Duration (min) 286.17 pH Buffer 7.0 7.0 Well Depth (ft) 114.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 66.45 Conductivity Dissolved DatefTime Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/19/2022 13:17 64.44 7965 4.20 15.40 475 4.5 10.0 10/19/2022 13:18 64.66 7946 4.23 15.33 477 4.0 9.0 10/19/2022 13:19 64.88 7935 4.24 15.34 478 4.0 8.8 10/19/2022 13:20 65.10 7918 4.24 15.30 479 3.9 8.5 Pumping Rate Calculations !volume of water purged (gals) 65.10 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 300.00 I Final Depth to Water (feet) 96.95 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Anal~ical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: I Arrived on site at 0815. Purge began at 0820. Purged well for a total of 300 minutes. Purge ended and samples collected at 1320. Water was clear. Left site at 1330. Signature of Field Technician ~ur~#~ Y-::.! ·.----J. "... -s .• ~ y..-==:c, -_, .. .r ~ ' Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) DatefTime Gallons Purged (gal) 10/13/2022 11:30 24.96 11/1/2022 12:45 11/1/2022 12:53 [volume of water purged (ga.ls) [Final Depth to Water (feet) Name of Certified Analytical Laboratory AWSL Anal~ical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals -Full Suite voes -Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater ,------------------,-----------------------, MW-23 Sampling Program MW-23 11012022 Sampling Event 2022 Q4 GW Quarterly 10/13/2022 9:30 11/1/2022 12:45 [sampler TH/DL Pump Weather Conditions Sunny QED External Ambient Temperature (C) 12 2 Casings Previous Well Sampled MW-26 11.81 113.64 7.0 Well Depth (ft) 132.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 113.90 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp {deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3966 7.00 18.50 344 1.0 59.8 3969 6.60 14.51 Before 3967 6.62 14.45 After Pumping Rate Calculations 24.96 Flow Rate (Q = S/60) (gal/min) .208 Time to evacuate 2 Casing Volumes (min) 120.00 129.34 Number of casing Volumes 2.00 Volume, if well evacuated to dryness (gals) 24.96 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE u 4 DegC y y WATER 1 250-ml HOPE y HN03 (pH<2) y y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-ml HDPE u 4 DegC y y WATER 1 250-ml HOPE y HN03 y Arrived on site at 0925. Purge began at 0930. Purged well for a total of 120 minutes. Purged well dry. Purge ended at 1130. Water was mostly clear. Left site at 1132. Arrived on site at 1240. Depth to water was 118.41. Samples collected at 1245. Left site at 1254. Signature of Field Technician ~~? Groundwater Discharge Permit ~ . ..- ;<,~ ' ~~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-24 ----, Sameling Program Field Sample ID MW-24 11022022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 11/1/2022 10:03 Sample Date & Time 11/2/2022 6:45 [~al'll_eler TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 11 Purging Method 2 Casings Previous Well Sampled MW-38 Casing Volume (gal) 7.19 Calculated Casing Volumes Purge Duration (min) 74.95 pH Buffer 7.0 7.0 Well Depth (ft) 120.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 108.98 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before / After 11/1/2022 11:25 15.36 4332 5.36 14.10 399 2.0 72.0 11/2/2022 6:45 4461 4.36 15.70 Before 11/2/2022 6:53 4478 4.39 15.73 After Pumping Rate Calculations [volume of water purged ig_als) 15.36 Flow Rate (Q = S/60) (gal/min) .192 Time to evacuate 2 Casing Volumes (min) 80.00 [ Final Depth to Water (feet) 116.80 Number of casing Volumes 2.00 Volume, if well evacuated to dryness (gals) 15.36 Name of Certified Analytical Laboratory AWSL Analy_tical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: minutes. Purge ater was clear. • ~v,,.,, ,v .. ~w, ·•~v , vv,vv. ~~,.,..,,vv vv .. vvwv v, 0645. Left site at 0655. Signature of Field Technician -=3~~ Groundwater Discharge Permit a ~ ' _,.,2 ~y~ , ., Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-24A Sampling Program Field Sample ID MW-24A 11022022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 11/1/2022 12:25 Sample Date & Time 11/2/2022 7:00 !sampler TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 11 Purging Method 2 Casings Previous Well Sampled MW-24 Casing Volume (gal) 7.75 Calculated Casing Volumes Purge Duration (min) 80.74 pH Buffer 7.0 7.0 Well Depth (ft) 122.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 110.13 Conductivity pH(pH Dissolved Date/Time Gallons Purged (umhos/cm) Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 11/1/2022 13:55 4574 4.90 15.30 423 1.4 90.9 11/2/2022 7:00 4441 4.50 14.23 11/2/2022 7:08 4453 4.52 14.25 Pumping Rate Calculations [volume of water purged (gals) 17.28 Flow Rate (Q = S/60) (gal/min) Time to evacuate 2 Casing Volumes (min) [Final Depth to Water (feet) 117.45 Number of casing Volumes Volume, if well evacuated to dryness (gals) Name of Certified Analytical Laboratory GEL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Gross Alpha y WATER 1 250-ml HOPE y HN03 Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C General lnorganics y WATER 1 250-ml HOPE u 4 Deg C Comments: Arrived on site at 1222. Purge began at 1225. Purged well for a totaT of g·o minutes. Purged well dry. Purge ended at 1355.-Water was clear. Left site at 1357. Arrived on site at 0656. Depth to water was 110.06. Samples collected at 0700. Left site at 0710. Signature of Field Technician ~~~ Before After .192 90.00 2.00 17.28 Added? y y y y y y Groundwater Discharge Permit ·w;=·' !::91----r ,.--f ' .• I'-/~ ~ .. -' ~· Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-25 Sampling Program Field Sample ID MW-25 10102022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 10/10/2022 7:20 Sample Date & Time 10/10/2022 10:40 I sampler I TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 10 Purging Method 2 Casings Previous Well Sampled N/A Casing Volume (gal) 21.46 Calculated Casing Volumes Purge Duration (min) 197.82 pH Buffer 7.0 7.0 Well Depth (ft) 115.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 82.13 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 10/10/2022 10:37 42.74 2801 6.46 3182 408 72.0 4.3 10/10/2022 10:38 42.96 2780 6.49 15.32 407 76.0 4.3 10/10/2022 10:39 43.18 2769 6.52 15.20 407 74.0 4.4 10/10/2022 10:40 43.40 2730 6.54 14.10 406 76.0 4.4 Pumping Rate Calculations [volume of wa_!er purged (gals) 43.40 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 200.00 I Final Depth to Water (feet) 85.05 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HNO3 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H25O4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HNO3 y Comments: Arrived on site at 0715. Purge began at 0720. Purged well for a total of 200 minutes. Purge ended and samples coliected at 1040. Water was clear but had tiny little bubbles surfacing. Left site at 1051 . Sianature of Field Technician --:3~~ I Groundwater Discharge Permit F-:, ... ··, ... 'I, .: ' " . ' ~ ,• E.NERGYFVELS Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater .------------------.-------------------------, Location ID MW-26 Sampling Program Field Sample ID MW-26 10132022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 10/13/2022 8:44 Sample Date & Time 10/13/2022 8:45 !sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type Grundfos External Ambient Temperature (C) 10 Purging Method 2 Casings Previous Well Sampled MW-12 Casing Volume (gal) 28.79 Calculated Casing Volumes Purge Duration () pH Buffer 7 .0 7.0 Well Depth (ft) 121.33 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 77.23 Conductivity Dissolved Date/Time Gallons Purged (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 10/13/2022 8:45 3500 6.40 13.57 397 0 26.3 !volume of water purged() Pumping Rate Calculations Flow Rate (Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes () I Final Depth to Water (feet) 110.34 Number of casing Volumes Volume, if well evacuated to dryness() 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 DegC y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: [Arrived on site at 0840. ~amples collected at 0845. Water was clear. Left site at 0850. Signature of Field Technician ~~~ Groundwater Discharge Permit ·' Groundwater Monitoring Quality Assurance Plan ,· ~ White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-27 Sampling Program Field Sample ID MW-27 10192022 Sampling Event 2022 Q4 GW Quarterly_ Purge Date & Time 10/19/2022 10:30 Sample Date & Time 10/19/2022 14:30 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 15 Purging Method 2 Casings Previous Well Sampled MW-22 Casing Volume (gal) 23.57 Calculated Casing Volumes Purge Duration (min) 217.26 pH Buffer 7 .0 7.0 Well Depth (ft) 95.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 58.90 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/19/2022 14:27 51.42 1225 7.08 15.36 399 10.0 97.1 10/19/2022 14:28 51.64 1223 7.09 15.21 394 9.0 97.0 10/19/2022 14:29 51.86 1215 7.13 15.18 391 8.7 96.7 10/19/2022 14:30 52.08 1217 7.15 15.17 389 8.4 96.0 [volume of water purged (gals) Pum_ei'!9_ Rate Calculations 52.08 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 240.00 [Fina!_D_E!e_th to Water (feet) 60.48 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: [ Arrived on site at 1026. Purge began at 1030. Purged well for a total of 240 minutes. Purg_e ended and samples collected at 1430. Water was clear. Left site at 1440. Signature of Field Technician ~~-17?-~~ Groundwater Discharge Permit VE:., .I ,.-.. r ---:-. ...---,, •' . ii ~y ~ S" . ~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-28 Sampling Program Field Sample ID MW-28 10122022 Sameli'!g Event 2022 Q4 GW Quarterly Purge Date & Time 10/12/2022 10:10 Sample Date & Time 10/12/2022 13:50 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 15 Purging Method 2 Casings Previous Well Sampled MW-15 Casing Volume (gal) 23.10 Calculated Casing Volumes Purge Duration (min) 212.99 pH Buffer 7.0 7.0 Well Depth (ft) 110.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 74.61 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/12/2022 13:47 47.08 4227 6.20 15.60 398 0 28.9 10/12/2022 13:48 47.30 4240 6.23 15.50 398 0 28.0 10/12/2022 13:49 47.52 4229 6.25 15.53 397 0 28.3 10/12/2022 13:50 47.74 4223 6.26 15.50 397 0 28.3 Pumping Rate Calculations [volume of water purged (gals) 47.74 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 220.00 [Final Depth to Water (feet) 77.12 Number of casing Volumes 2.00 Volume, if well evacuated to dryness O 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2}, 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HNO3 y Comments: [ Arrived on site at 1007. Purge began at 1010. PLJrged well for a total of 220 minutes. Purge ended and samples collected at 1350, Water was clear. Left site at 1400. Signature of Field Technician --:3~~ F-:·.-~ r.; ' , -,~~y~<; ~~- Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date!Time Gallons Purged (gal) 10/12/2022 9:52 10/12/2022 9:53 10/12/2022 9:54 10/12/2022 9:55 [volume of water pur!:Jed (gals) [ Final Depth to Water (feet) 38.40 38.62 38.84 39.06 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals -Full Suite voes -Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-29 Sampling Program MW-29 10122022 Sampling Event 2022 Q4 GW Quarterly 10/12/2022 6:55 10/12/2022 9:55 !sampler TH/DL Pump Weather Conditions Sunny QED External Ambient Temperature (C) 8 2 Casings Previous Well Sampled MW-36 18.39 169.53 7.0 Well Depth (ft) 135.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 106.83 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4564 6.37 14.71 248 7.2 6.3 4575 6.37 14.68 244 7.6 6.0 4574 6.37 14.68 240 7.4 6.0 4577 6.38 14.68 238 7.5 5.8 Pumping Rate Calculations 39.06 Flow Rate (Q :: S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 180.00 109.38 Number of casing Volumes 2.00 Volume, if well evacuated to dryness O 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-mL HOPE u 4 Deg C y y WATER 1 250-mL HOPE y HN03 (pH<2) y y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y y WATER 1 250-mL HOPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-mL HOPE u 4 Deg C y y WATER 1 250-mL HOPE y HN03 y [Arrived ()_h site at 0650. Pu_r_ge began at 0655. Purged well for a total of 180 minutes. Purge ended and samples collected at 0955. Water was clear. Left site at 1005. Signature of Field Technician -:3~, Groundwater Discharge Permit .• ·v;:· -' r ..... : ,/ ,=,--=r,;s; ~~ ... '/ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-30 Sampling Program Field Sample ID MW-30 10132022 Sampling Event 2022 Q4 GW Quarterly_ Purge Date & Time 10/13/2022 6:40 Sample Date & Time 10/13/2022 10:10 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 10 Purging Method 2 Casings Previous Well Sampled MW-05 Casing Volume (gal) 22.58 Calculated Casing Volumes Purge Duration (min) 208.11 pH Buffer 7.0 7.0 Well Depth (ft) 110.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 75.42 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/13/2022 10:07 44.91 2267 6.77 14.49 337 0 54.0 10/13/2022 10:08 45.13 2257 6.78 14.53 336 0 54.0 10/13/2022 10:09 45.35 2249 6.80 14.55 334 0 53.0 10/13/2022 10:10 45.57 2247 6.84 14.51 334 0 53.7 Pumping Rate Calculations [volume of wat~ purged (gals) 45.57 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 [Final Depth to Water_(feet) 76.24 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical ~_inples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: [Arrived on site at 0635. Purge began at 0640. Purged well for a total of 210 minutes, Purge ended and sami)_les collected at 1010. Water was clear. Left site at 1020. Signature of Field Technician ~~ Groundwater Discharge Permit ~F-:·~.,./ s _.,r~Y~ f . .• - Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-31 Sampling Program Field Sample ID MW-31 10112022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 10/11/2022 7:00 Sample Date & Time 10/11/2022 13:10 I sampler I TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 9 Purging Method 2 Casings Previous Well Sampled MW-32 Casing Volume (gal) 39.48 Calculated Casing Volumes Purge Duration (min) 363.93 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 69.53 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/11/2022 13:07 79.63 3405 7.06 16.40 327 388 113.0 10/11/2022 13:08 79.85 3393 7.05 15.24 324 360 113.0 10/11/2022 13:09 80.07 3389 7.03 15.39 323 378 112.0 10/11/2022 13:10 80.29 3399 7.01 15.40 321 379 112.0 Pumping Rate Calculations jvolume of water purged (gals) 80.29 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 370.00 I Final Depth to Water (feet) 73.85 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 DegC y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: Arrived on site at 0655. Purge began at 0700. Purged well for a total of 370 minutes. Purge ended and samples collected at 1310. Water was clear but had tiny little bubbles surfacing . Left site at 1320. Signature of Field Technician --=3~~ I Groundwater Discharge Permit ,• c=-.,~. .r / ~/ .,.-~YFVELS Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-32 Sampling Program Samplin_g Program Field Sample ID MW-32 10112022 Sampling Event Sampling Event 2022 Q4 GW Quarterly 2022 Q4 GW Quarterly Purge Date & Time 10/11/2022 6:45 Sample Date & Time 10/11/2022 11:45 !sampler !sampler I TH/DL TH/DL I Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 9 Purging Method 2 Casings Previous Well Sampled MW-11 Casing Volume (gal) 31.23 Calculated Casing Volumes Purge Duration (min) 287.86 pH Buffer 7.0 7.0 Well Depth (ft) 130.60 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 82.77 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/11/2022 11:42 64.44 3707 6.20 14.88 226 10.0 5.0 10/11/2022 11:43 64.66 3697 6.21 14.85 219 11.0 5.0 10/11/2022 11:44 64.88 3696 6.22 14.83 216 12.0 4.9 10/11/2022 11:45 65.10 3702 6.23 14.84 215 12.1 4.9 Pumping Rate Calculations [volume of water purged (gals) 65.10 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 300.00 jFinal Depth to Water (feet) 88.82 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HNO3 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-mL HDPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HNO3 y Comments: [ Arrived on site at 0640. Pu_r-_ge began at 0645. Purged well for a total of 300 minutes. Purge ended and samples collected at 1145. Water was a little murky. Left site at 1155. Signature of Field Technician ~«~/4-a;:...: ~~ --,'11:f: ~~YFLeo/ S Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 10/31/2022 12:57 64.44 10/31/2022 12:58 64.66 10/31/2022 12:59 64.88 10/31/2022 13:00 65.10 [volume of water__purged (gals) [ Final Depth to Water (feet) Name of Certified Analytical Laboratory GEL Analytical Samples Information Type of Sample/Analysis Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-32 Sampling Program MW-32 10312022 Sampling Event 2022 GW MW-32 Resample 10/31/2022 8:00 10/31/2022 13:00 [sampler TH/DL Pump Weather Conditions Clear QED External Ambient Temperature (C) 3 2 Casings Previous Well Sampled N/A 31.12 286.83 7.0 Well Depth (ft) 130.60 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 82.94 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 3691 6.10 14.76 203 38.0 13.8 3717 6.12 14.70 203 38.0 12.0 3717 6.15 14.67 203 39.0 11.5 3720 6.17 14.63 202 39.0 11.3 Pumping_ Rate Calculations 65.10 Flow Rate (Q = S/60} (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 300.00 88.75 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number I Type Sample Filtered? Type I Added? y WATER 1 I 250-mL HOPE y HNO3 I y I Arrived on site at 0755. Purge began at 0800. Purged well for a total of 300 minutes. Purge ended and sample collected at 1300. Water was murky. Left site at 1303. Signature of Field Technician --:3~~ Groundwater Discharge Permit -· -'~Wf:v ,; .-~ -=:ir:s . . , -, ' -· . ~y~ 'I -l ,•' ~~ " , ____ , Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-35 Sampling Program Field Sample ID MW-35 10312022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 10/31/2022 12:30 Sample Date & Time 10/31/2022 13:45 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 11 Purging Method 2 Casings Previous Well Sampled MW-02 Casing Volume (gal) 8.01 Calculated Casing Volumes Purge Duration (min) 73.84 pH Buffer 7.0 7.0 Well Depth (ft) 124.50 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 112.23 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/31/2022 13:42 15.62 4124 6.45 15.00 325 0 8.0 10/31/2022 13:43 15.84 4137 6.48 14.81 313 0 7.8 10/31/2022 13:44 16.05 4150 6.50 14.70 306 0 7.4 10/31/2022 13:45 16.27 4147 6.51 14.65 300 0 7.3 Pumping Rate Calculations [volume of water purged (gals) 16.27 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 75.00 [ Final Depth to Water (feet) 112.98 Number of casing Volumes 2.00 Volume, if well evacuated to dryness O 0 Name of Certified Analytical Laboratory AWSL Analytic_aJ Samples Information Sample Container Preservative Type of Sample/ Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-mL HDPE y HNO3 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-mL HDPE u 4 Deg C y Gross Alpha y WATER 1 250-mL HDPE y HNO3 y Comments: [ Arrived on sit_e at 1225. Purge began at 1230. Purged well for a total of 75 minutes. Purge ended and samples collected at 1345. Water was clear. Left site at 1400. Signature of Field Technician -:3 ....,.___..,,-,,,...~ Groundwater Discharge Permit ·w;;:~. I. ~s r.; -. ~~ ··r ~ . l Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-36 Sampling Program Field Sample ID MW-36 10112022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 10/11/2022 13:25 Sample Date & Time 10/11/2022 14:35 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 21 Purging Method 2 Casings Previous Well Sampled MW-14 Casing Volume (gal) 7.30 Calculated Casing Volumes Purge Duration (min) 67.28 pH Buffer 7.0 7.0 Well Depth (ft) 121.60 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 110.42 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 10/11/2022 14:32 14.53 4580 6.68 15.20 375 0 75.0 10/11/2022 14:33 14.75 4694 6.70 15.15 374 0 74.0 10/11/2022 14:34 14.97 4673 6.71 15.12 373 0 75.0 10/11/2022 14:35 15.19 4680 6.73 15.10 371 0 75.0 Pumping Rate Calculations - [volume of water purged (gals) 15.19 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 70.00 [Final Depth to Wat~(feet}_ 111.09 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HNO3 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HNO3 y Comments: [ Arrived on site at 1322. Purge began at 1325. Purged well for a total of 70 minutes. Purge ended and samples collected at 1435. Left site at 1445. Water was clear. Signature of Field Technician ~~ Groundwater Discharge Permit ~-a-··•-~~ .. __ :'; -~~y __. .•. Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-37 Sampling Program Field Sample ID MW-37 11012022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 10/14/2022 9:30 Sample Date & Time 11/1/2022 13:05 I sampler TH/DL Purging Equipment Bailer Weather Conditions Sunny Pump Type Grundfos External Ambient Temperature (C) 13 Purging Method 2 Casings Previous Well Sampled MW-23 Casing Volume O 10.35 Calculated Casing Volumes Purge Duration O pH Buffer 7.0 7.0 Well Depth (ft) 121.80 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 105.95 Conductivity Dissolved Date!Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/14/2022 9:38 5.00 4372 6.12 14.41 428 17.6 72.0 11/1/2022 13:05 4840 6.60 14.20 11/1/2022 13:08 4816 6.60 14.15 !Volume of water purged (gals) Pumping Rate Calculations 15.00 Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes O I Final D~pth to Water (feet) 121.49 Number of casing Volumes Volume, if well evacuated to dryness (gals) Name of Certified Analytical Laboratory AWSL Analytical Sameles Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Total Dissolved Soilds y WATER 1 250-mL HDPE u 4 Deg C Heavy Metals -Full Suite y WATER 1 250-mL HDPE y HNO3 (pH<2) VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C Nutrients y WATER 1 250-mL HDPE u H25O4 (pH<2), 4 Deg C General lnorganics y WATER 1 250-mL HDPE u Gross Alpha y WATER 1 250-mL HDPE y Comments: Arrived on site at 0924. Bailing began at 0930. Bailed a total of 15 gallons from well. Bailed well dry. Water was a little murky. Left site at 0956. Arrived on site at 1300. Depth to water was 113.15. Samples bailed and collected at 1305. Left site at 1310. Signature of Field Technician --=--, I J-·. //"~ ----J.✓ '~.F!,,p __ (__, -,. ,...Fl-:.. ~--·?") 4 Deg C HNO3 Before After 15.00 Added? y y y y y y 2F-::·/ ,·~.,· .• ;~ V ' f ENERGYFVEZ..S Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration () pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) White Mesa Mill / Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan Field Data Worksheet For Groundwater MW-38 Sampling Program MW-38 11012022 Sampling Event 11/1/2022 7:30 11/1/2022 12:30 lsamr:>_ler Bailer Weather Conditions External Ambient Temperature (C) 2 Casings Previous Well Sampled 2.78 7.0 Well Depth (ft) 4.0 Well Casing Diameter (in) 1000 Depth to Water Before Purging (ft) Conductivity 2022 Q4 GW Quarterly TH/DL Clear 2 MW-35 74.40 4 70.14 Dissolved DatefTime Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 11/1/2022 7:35 5.00 4064 6.65 14.60 376 11/1/2022 12:30 4317 6.25 14.40 11/1/2022 12:34 4300 6.30 14.32 Pumping Rate Calculations ~u'!le ~f water purg~d (gals) 5.00 Flow Rate (Q = S/60) O !Final Depth to Water (feet) 74.35 Time to evacuate 2 Casing Volumes () Number of casing Volumes Volume, if well evacuated to dryness (gals) Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Type of Sample/ Analysis Collected? Matrix Number Type Sample Filtered? Total Dissolved Soilds y WATER 1 250-ml HDPE u Heavy Metals -Full Suite y WATER 1 250-ml HOPE y VOCs -Full Suite for GW y WATER 3 40mlVOA u Nutrients y WATER 1 250-ml HDPE u General lnorganics y WATER 1 250-ml HDPE u Gross Alpha y WATER 1 250-ml HDPE y Comments: Arrived on site at 0725. Bailing began at 0730. Balled a total of 5 gallons from well. Bailed well dry. Water was murky. Left site at 0738. Arrived on site at 1225. Depth to water was 70.51 . Samples bailed and collected at 1230. Left site at 1235. Signature of Field Technician ~~~ 133.0 87.0 Before After 1.79 5.00 Preservative Type Added? 4 DegC y HN03 (pH<2) y HCI (pH<2), 4 Deg C y H2S04 (pH<2), 4 Deg C y 4 DegC y HN03 y ~~·Y, ~-,·__,..~~ ~•",::_ ~ )' Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 10/20/2022 10:27 51.42 10/20/2022 10:28 51.64 10/20/2022 10:29 51.86 10/20/2022 10:30 52.08 [volume of water purged (galsJ [ Final Depth to Water (feet) Name of Certified Analytical Laboratory AWSL Anal~ical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals -Full Suite voes -Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-39 Sampling Program Sampling Program MW-39 10202022 Sampling Event Sampling Event 2022 Q4 GW Quarterly 2022 Q4 GW Quarterly 10/20/2022 6:30 10/20/2022 10:30 I sampler [~ampler I TH/DL TH/DL Pump Weather Conditions Clear QED External Ambient Temperature (C) 6 2 Casings Previous Well Sampled MW-27 24.89 229.42 7.0 Well Depth (ft) 102.50 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 64.38 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 4773 3.95 14.70 429 0 3.5 4794 3.96 14.65 436 0 3.5 4797 3.97 14.62 442 0 3.4 4798 3.97 14.65 449 0 3.5 Pumping_ Rate Calculations 52.08 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 240.00 69.72 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE u 4 Deg C y y WATER 1 250-ml HOPE y HNO3 (pH<2) y y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u H2SO4 (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u 4 Deg C y y WATER 1 250-ml HOPE y HNO3 y [ Arrived on site at 0625. Purge began at 0630. Purged well for a total of 240 minutes. Purge ended and samples collected at 1030. Water was clear. Left site at 1040. Signature of Field Technician -=3C,(.JlJ\..I.-A:..-,c I Groundwater Discharge Permit e ··F-::·'/ ~ ~ _.· ~ 'I _ ~,r .:-~ E7tJIERJG'Y~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-39 Sampling Program Field Sample ID MW-39 11012022 Sampling Event 2022 MW-02 and MW-39 Resample Purge Date & Time 11/1/2022 7:20 Sample Date & Time 11/1/2022 11:20 [sampler TH/DL Purging Equipment Pump Weather Conditions Clear Pump Type QED External Ambient Temperature (C) 2 Purging Method 2 Casings Previous Well Sampled MW-32 Casing Volume (gal) 25.00 Calculated Casing Volumes Purge Duration (min) 230.44 pH Buffer 7.0 7.0 Well Depth (ft) 102.50 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 64.21 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 11/1/2022 11:17 51.42 4840 4.20 14.46 391 0 5.4 11/1/2022 11:18 51.64 4837 4.18 14.50 390 0 5.2 11/1/2022 11:19 51.86 4832 4.15 14.52 392 0 5.0 11/1/2022 11:20 52.08 4837 4.13 14.52 395 0 5.0 Pumping Rate Calculations [volume of water purged (gals) 52.08 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 240.00 [ Final Depth to Water (feet) 68.64 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory GEL Analytical Samples Information Sample Container Preservative Type of Sample/ Analysis Collected? Matrix Number I Type Sample Filtered? Type I Added? Gross Alpha y WATER 1 I 250-ml HOPE y HN03 I y Comments: [ Arrived on site at 0715. Purge began at 0720. Purged well for a total of 240 minutes. Purge ended and samples collected at 1120. Water was clear. Left site at 1124. Signature of Field Technician ~uJVV~ Groundwater Discharge Permit w;::I ,/ IF; r f i -i r ~YF'l,;-s,; S Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-40 Sampling Program Sampling Program Field Sample ID MW-40 10182022 Sampling Event Sampling Event 2022 Q4 GW Quarterly 2022 Q4 GW Quarterly Purge Date & Time 10/18/2022 7:15 Sample Date & Time 10/18/2022 11:20 I sampler [sampler I TH/DL TH/DL I Purging Equipment Pump Weather Conditions Clear Pump Type QED External Ambient Temperature (C) 6 Purging Method 2 Casings Previous Well Sampled MW-18 Casing Volume (gal) 26.17 Calculated Casing Volumes Purge Duration (min) 241.27 pH Buffer 7.0 7.0 Well Depth (ft) 120.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 79.91 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 10/18/2022 11:17 52.51 3899 6.74 15.01 425 3.0 110.0 10/18/2022 11:18 52.73 3899 6.70 14.91 424 3.0 110.0 10/18/2022 11:19 52.94 3895 6.70 14.90 423 2.9 111.0 10/18/2022 11:20 53.16 3900 6.71 14.88 422 2.9 111.0 Pumping Rate Calculations [volume of water purged (gals) 53.16 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 245.00 [Final ~ept_!I to Water (feet) 80.74 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HNO3 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: !Arrived on site at 0710. Purge began at 0715. Purged well for a total of 245 minutes. Purge ended and samples collected at 1120. Water was clear. Left site at 1130. Signature of Field Technician ~~~ Groundwater Discharge Permit ew;::-·· ~· .-· .. ,'· /~y~s I .• ' ' , Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID TW4-24 Sampling Program Field Sample ID TW4-24 11012022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time 11/1/2022 13:29 Sample Date & Time 11/1/2022 13:30 [sampler TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type Grundfos External Ambient Temperature (C) 12 Purging Method 2 Casings Previous Well Sampled MW-24A Casing Volume (gal) 31.27 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 114.80 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 66.91 Conductivity Dissolved Date/Time Gallons Purged (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 11/1/2022 13:30 7020 6.46 15.42 340 0 21.0 Pumping Rate Calculations [volume of water purged() Flow Rate (Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes () ~al [)~pth to Water (feet) 70.45 Number of casing Volumes Volume, if well evacuated to dryness O 0 Name of Certified Analytical Laboratory GEL Analytical Samples Information Sample Container Preservative Type of Sample/ Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Gross Alpha y WATER 1 250-ml HDPE y HNO3 y Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HNO3 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 DegC y Comments: [ Arrived on site at 1326. Samples collected at 1330. Water was clear. Left site at 1335. Signature of Field Technician ~~~ Groundwater Discharge Permit ~y~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-65 Sampling Program Field Sample ID MW-65 10132022 Sampling Event 2022 Q4 GW Quarterly Purge Date & Time Sample Date & Time 10/13/2022 9:05 I sampler TH/DL Purging Equipment ' Weather Conditions Pump Type External Ambient Temperature () Purging Method Previous Well Sampled Casing Volume O Calculated Casing Volumes Purge Duration () pH Buffer 7.0 Well Depth (ft) pH Buffer 4.0 Well Casing Diameter() Specific Conductance () Depth to Water Before Purging (ft) Date/Time Gallons Purged Conductivity J)_H Teme Redox Turbidity Dissolved Oxygen I Before/After ] Pumein_g_ Rate Calculations [volume of water purged _O Flow Rate (Q = S/60) O Time to evacuate 2 Casing Volumes () [ Final pepth to Water (feet) Number of casing Volumes Volume, if well evacuated to dryness () Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4DegC y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HNO3 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 DegC y Gross Alpha y WATER 1 250-ml HDPE y HNO3 y Comments: Duplicate of MW-12 Signature of Field Technician ~ F-, !!!'llai 1', . ...,. :r:; ,. _ EAIERGYFVEZ.S Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume () Calculated Casing Volumes Purge Duration () pH Buffer 7 .0 pH Buffer 4.0 Specific Conductance O Date/Time Gallons Purged [volume of water purged() jFinal Depth to Water (feet) Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: I Duplicate of MW-35 Signature of Field Technician ~~~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-70 Sampling Program MW-70 10312022 Sampling Event 2022 Q4 GW Quarterly 10/31/2022 13:45 [sampler TH/DL Weather Conditions External Ambient Temperature () Previous Well Sampled Well Depth (ft) Well Casing Diameter () Depth to Water Before Purging (ft) Dissolved Conductivity pH Temp Redox Turbidity Oxygen I Before/After Pumpin_g_ Rate Calculations Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () Number of casing Volumes Volume, if well evacuated to dryness () Container Preservative ~mple Collectec Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-mL HOPE u 4 Deg C y y WATER 1 250-mL HOPE y HN03 (pH<2) y y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y y WATER 1 250-mL HOPE u H2504 (pH<2), 4 Deg C y y WATER 1 250-mL HOPE u 4DegC y y WATER 1 250-mL HOPE y HN03 y TabC Field Data Worksheets Accelerated Monitoring Tab Cl Field Data Worksheets Accelerated Monitoring November 2022 Groundwater Discharge Permit ~ Groundwater Monitoring Quality Assurance Plan ' V White Mesa Mill ~-~Y~S Field Data Worksheet For Groundwater Location ID MW-11 Saml)ling Prog_ram Field Sample ID MW-11 11082022 Sampling Event Purge Date & Time 11/8/2022 7:55 Sample Date & Time 11/8/2022 12:30 [sameler Purging Equipment Pump Weather Conditions Pump Type QED External Ambient Temperature (C) Purging Method 2 Casings Previous Well Sampled Casing Volume (gal) 29.31 Calculated Casing Volumes Purge Duration (min) 270.22 pH Buffer 7 .0 7.0 Well Depth (ft) pH Buffer 4.0 4.0 Well Casing Diameter (in) Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) Conductivity pH (pH Date!Time Gallons Purged (gal) (umhos/cm) Units) Temp (deg C) Redox (mV) 11/8/2022 12:27 59.02 3062 6.40 15.60 495 11/8/2022 12:28 59.24 3034 6.42 14.60 487 11/8/2022 12:29 59.45 3083 6.48 14.62 483 11/8/2022 12:30 59.67 3033 6.53 14.70 479 Pumping Rate Calculations !Volume of water purged (gals) 59.67 Flow Rate (Q = S/60) (gal/min) Time to evacuate 2 Casing Volumes (min) [Final Depth to Water (feet) 86.99 Number of casing Volumes Volume, if well evacuated to dryness O Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Chloride y WATER 1 500-ml Poly u Heavy Metals -Mn only y WATER 1 250-ml HOPE y Sulfate y WATER 1 250-ml HOPE u Total Dissolved Soilds y WATER 1 250-ml HOPE u Nitrate/nitrite as N y WATER 1 250-ml HOPE u Comments: Arrived on site at 0750. Purge began at 0755. Purged well for a total of 275 minutes. Purge ended and samples collected at 1230. Water was mostly clear with tiny little bubbles surfacin-9_. Left site at 1238. Signature of Field Technician ~~~ November Monthly_ TH/DL Partly cloudy 4 N/A 130.00 4 85.10 Dissolved Turbidity (NTU) Oxygen(%) Before/ After 10.0 9.0 11.0 7.0 12.0 6.5 12.3 6.3 .217 275.00 2.00 0 Preservative Type Added? None N HNO3 (pH<2) y None N 4 Deg C y H2SO4 (pH<2), 4 Deg C y Groundwater Discharge Permit ~ ). ,r V IP": , ~.-,..~ ~•r ~Y~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-25 Sampling Program Field Sample ID MW-25 11092022 Sampling Event November Monthly Purge Date & Time 11/9/2022 7:10 Sample Date & Time 11/9/2022 11:10 [sampler .TH/DL Purging Equipment Pump Weather Conditions Windy with rain Pump Type QED External Ambient Temperature (C) 9 Purging Method 2 Casings Previous Well Sampled MW-30 Casing Volume (gal) 21.71 Calculated Casing Volumes Purge Duration (min) 200.11 pH Buffer 7.0 7.0 Well Depth (ft) 115.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 81.75 pH (pH Dissolved DatefTime Gallons Purged (gal) Conductivity (umhos/cm) Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 11/9/2022 11:07 51.42 3220 6.46 14.20 469 0 2.2 11/9/2022 11:08 51.64 3229 6.50 14.16 466 0 2.0 11/9/2022 11:09 51.86 3222 6.52 14.10 464 0 1.9 11/9/2022 11:10 52.08 3218 6.55 14.09 463 0 1.8 Pumping Rate Calculations [volume of water purged (gal~ 52.08 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 240.00 [ Final Depth to Water (feet) 83.56 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number I Type Sample Filtered? Type I Added? Total Dissolved Soilds y WATER 1 T 250-ml HOPE u 4 Deg C I y Comments: [ Arrived on site at 070~rge began at 0710. Purged well for a total of 240 minutei_s. Purge ended and samples collected at 1110. Water was clear. Left site at 1113. Signature of Field Technician ~t.U"~TO~~ Groundwater Discharge Permit Vf;:r-.,.i .,. f ~-~l ~YFVJEL.S Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-26 Sampling Program Field Sample ID MW-26 11102022 Sampling Event November Monthly Purge Date & Time 11/10/2022 7:14 Sample Date & Time 11/10/2022 7:15 !sampler TH/DL Purging Equipment Pump Weather Conditions Clear Pump Type Grundfos External Ambient Temperature (C) -1 Purging Method 2 Casings Previous Well Sampled MW-25 Casing Volume (gal) 28.86 Calculated Casing Volumes Purge Duration () pH Buffer 7 .0 7.0 Well Depth (ft) 121.33 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 77.12 Conductivity Dissolved Date/Time Gallons Purged (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 11/10/2022 7:15 3511 6.38 15.27 461 0 30.7 Pumping Rate Calculations !volume of water purged () Flow Rate (Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes () [Final Depth to Water (feet) 94.49 Number of casing Volumes Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y voes-Chloroform y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Comments: [Arrived on site at 0710. Samples collected at 0715. Water was clear. Left site at 0722. Signature of Field Technician ~~r~~~ Groundwater Discharge Permit -----.~,' IF: ·' ' ~· V ~Y,11C;L451" s . I Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-30 Sampling Program Field Sample ID MW-30 11092022 Sampling Event November Monthly Purge Date & Time 11/9/2022 7:00 Sample Date & Time 11/9/2022 10:35 [sampler TH/DL Purging Equipment Pump Weather Conditions Windy with rain Pump Type QED External Ambient Temperature (C) 9 Purging Method 2 Casings Previous Well Sampled MW-31 Casing Volume (gal) 22.90 Calculated Casing Volumes Purge Duration {min) 211.06 pH Buffer 7.0 7.0 Well Depth (ft) 110.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 74.93 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 11/9/2022 10:32 46.00 1895 6.30 14.73 473 0 52.0 11/9/2022 10:33 46.22 1945 6.34 14.69 469 0 52.0 11/9/2022 10:34 46.43 1978 6.35 14.74 466 0 51.5 11/9/2022 10:35 46.65 1998 6.37 14.60 464 0 51.0 Pumping Rate Calculations [volume of water purged (gals) 46.65 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 215.00 [Final Depth to Wat~r (feet) 75.99 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/ Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-mL Poly u None N Nitrate/nitrite as N y WATER 1 250-mL HDPE u H2SO4 (pH<2), 4 Deg C y Heavy Metals -U and Se only y WATER 1 250-mL HDPE y HN03 (pH<2) y Comments: [ Arrived on site at 0655. Purge began at 0700. Purged well for a total of 215 minutes. Purge en~d a_nd saml)_les collected at 1035. Water was clear. Left site at 1045. Signature of Field Technician --:3~ Groundwater Discharge Permit F-_.--r :, i,: { -_, . l ~y~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-31 Sampling Program Sampling Program Field Sample ID MW-31 11082022 Sampling Event Sampling Event November Monthly November Monthly Purge Date & Time 11/8/2022 8:10 Sample Date & Time 11/8/2022 14:20 !sampler [sampler I TH/DL TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 4 Purging Method 2 Casings Previous Well Sampled MW-11 Casing Volume (gal) 39.51 Calculated Casing Volumes Purge Duration (min) 364.23 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 69.48 Conductivity pH(pH Dissolved DatefTime Gallons Purged (gal) (um hos/cm) Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 11/8/2022 14:17 79.63 3475 6.40 14.80 479 100.2 113.4 11/8/2022 14:18 79.85 3472 6.46 14.70 472 112.0 113.1 11/8/2022 14:19 80.07 3486 6.50 14.65 470 114.0 112.9 11/8/2022 14:20 80.29 3487 6.53 14.76 467 115.0 113.0 Pumping Rate Calculations [volume of water purged (gals) 80.29 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 370.00 [ Final Depth to Water (fe~t) 75.21 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-mL Poly u Nitrate/nitrite as N y WATER 1 250-mL HDPE u Sulfate y WATER 1 250-mL HDPE u Total Dissolved Soilds y WATER 1 250-mL HOPE u Heavy Metals -U only y WATER 1 250-mL HDPE y Comments: Arrived on site at 0805. Purge began at 0810. Purged well for a total of 370 minutes. Purge ended and samples collected at 1420. Water was mosUy clear with tiny lit!le bubbles surfacing. Left site at 1428. Signature of Field Technician ~ None N H2S04 (pH<2), 4 Deg C y None N 4 Deg C y HN03 (pH<2) y I Groundwater Discharge Permit F-/ t . r/ °7 'r~y~s . _I Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-65 Sampling_ Program Field Sample ID MW-65 11092022 Sampling Event November Monthly Purge Date & Time Sample Date & Time 11/9/2022 10:35 !sampler TH/DL Purging Equipment Weather Conditions Pump Type External Ambient Temperature () Purging Method Previous Well Sampled Casing Volume () Calculated Casing Volumes Purge Duration () pH Buffer 7 .0 Well Depth (ft) pH Buffer 4.0 Well Casing Diameter () Specific Conductance () Depth to Water Before Purging (ft) I l l Dissolved l Before/After Date/Time Gallons Purged Conductivity pH Temp Redox Turbidity Oxygen Pumping Rate Calculations [volume of water purged() Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () [Final Depth to Water (feet) Number of casing Volumes Volume, if well evacuated to dryness () Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y Heavy Metals -U and Se only y WATER 1 250-ml HDPE y HNO3 (pH<2) y Comments: [Duplicate of MW-30 Signature of Field Technician ~~~ TabC2 Field Data Worksheets Accelerated Monitoring December 2022 Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill ~V-F~ Field Data Worksheet For Groundwater Location ID MW-11 Sampling_frogram Field Sample ID MW-11 12142022 Sampling Event December Monthly Purge Date & Time 12/14/2022 7:40 Sample Date & Time 12/14/2022 12:15 jsampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) -4 Purging Method 2 Casings Previous Well Sampled MW-30 Casing Volume (gal) 29.35 Calculated Casing Volumes Purge Duration (min) 270.00 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 85.04 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 12/14/2022 12:12 59.02 3172 7.01 13.80 367 0 1.0 12/14/2022 12:13 59.24 3177 7.05 13.82 365 0 1.0 12/14/2022 12:14 59.45 3173 7.08 13.84 364 0 1.0 12/14/2022 12:15 59.67 3167 7.10 13.83 363 0 1.0 Pumping Rate Calculations [volume of water purged (gals) 59.67 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 275.00 [Final Depth to Wate!Jfeet) 85.23 Number of casing Volumes 2.00 Volume, if well evacuated to dryness() 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Heavy Metals -Mn only y WATER 1 250-ml HOPE y HN03 (pH<2) y Sulfate y WATER 1 250-ml HOPE u None N Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 DegC y Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y Comments: [ Arrived on site at 0735. Purge began at 07 40. Purged well for a total 275 minutes. Purg_e ended and samples collected at 1215. Water was clear. Left site at 1221. Signature of Field Technician ~ ' ) Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill ~~ Field Data Worksheet For Groundwater Location ID MW-25 Sampling Program Field Sample ID MW-25 12142022 Sampling_ Event December Monthly Purge Date & Time 12/14/2022 8:15 Sample Date & Time 12/14/2022 11:45 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) -4 Purging Method 2 Casings Previous Well Sampled MW-11 Casing Volume (gal) 21.61 Calculated Casing Volumes Purge Duration (min) 199.21 pH Buffer 7.0 7.0 Well Depth (ft) 115.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 81.90 Conductivity Dissolved Date/Time Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 12/14/2022 7:15 45.57 3206 6.54 14.25 410 0 4.5 12/14/2022 11:42 44.91 3210 6.40 14.30 410 0 4.7 12/14/2022 11:43 45.13 3209 6.47 14.30 410 0 4.9 12/14/2022 11:44 45.35 3219 6.51 14.28 410 0 4.8 Pumping Rate Calculations [\,lolume of water purged (gals) 45.57 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 [Final Depth to Water (feet) 83.47 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number I Type Sample Filtered? Type I Added? Total Dissolved Soilds y WATER 1 I 250-mL HDPE u 4 Deg C I y Comments: I Arrived on site at 0810. Purge began at 0815. Purged well for a total of 210 minutes. Purge ended and samples collected at 1145. Water was clear. Left site at 1152. Signature of Field Technician -~. ~--,/, .-~ .. -,: <~.;..) "- Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-26 Sampling_ Program Field Sample ID MW-26 12152022 Sampling_ Event December Monthly Purge Date & Time 12/15/2022 7:59 Sample Date & Time 12/15/2022 8:00 [sampler TH/DL Purging Equipment Pump Weather Conditions Cloudy Pump Type Grundfos External Ambient Temperature (C) -4 Purging Method 2 Casings Previous Well Sampled MW-25 Casing Volume (gal) 28.50 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 121.33 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 77.67 Conductivity Dissolved Date/Time Gallons Purged (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 12/15/2022 7:59 3524 6.45 15.70 478 0 34.0 Pumping Rate Calculations [volume of water purged() Flow Rate (Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes () [ Final Depth to Water (feet) 101.46 Number of casing Volumes Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y voes-Chloroform y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Comments: [ Arrived on site at 0755. Samples collected at 0800. Water was clear. Left site at 0805. Signature of Field Technician ---, -----~ , -': .r-4-_,.,:___,.--/-:r ·:>~~<~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill ~ -Field Data Worksheet For Groundwater Location ID MW-30 Sampling Program Field Sample ID MW-30 12132022 Sampling Event December Monthly Purge Date & Time 12/13/2022 8:50 Sample Date & Time 12/13/2022 12:25 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) -8 Purging Method 2 Casings Previous Well Sampled MW-31 Casing Volume (gal) 22.93 Calculated Casing Volumes Purge Duration (min) 211.42 pH Buffer 7.0 7.0 Well Depth (ft) 110.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 74.87 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox(mV) Turbidity (NTU) Oxygen(%) Before/After 12/13/2022 12:22 47.08 2251 6.55 14.29 457 0 54.0 12/13/2022 12:23 47.30 2245 6.55 13.24 452 0 53.6 12/13/2022 12:24 47.52 2245 6.57 14.27 449 0 53.4 12/13/2022 12:25 47.74 2243 6.59 13.27 446 0 53.6 Pumping Rate Calculations \volume of water purged (gals) 47.74 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 220.00 [Final Depth to Water (feet) 76.13 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y Heavy Metals -U and Se only y WATER 1 250-ml HDPE y HN03 (pH<2) y Comments: [ Arrived on site at 0840. Purge began at 0845. Purged well for a total of 220 minutes. Purge ended and samples collected at 1225. Water was clear. Left site at 1237. Signature of Field Technician --, C /'/.: ~ .____).>:,'._I~✓• ,:_ ;~ >-. -.:_,t; ;~·-) Groundwater Discharge Permit ---~ ----=:--~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-31 Sampling Program Field Sample ID MW-31 12132022 Sampling Event December Monthly Purge Date & Time 12/13/2022 8:15 Sample Date & Time 12/13/2022 14:25 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) -8 Purging Method 2 Casings Previous Well Sampled N/A Casing Volume (gal) 39.72 Calculated Casing Volumes Purge Duration (min) 366.10 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 69.17 Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 12/13/2022 14:22 79.63 3514 6.70 14.20 432 0 111.1 12/13/2022 14:23 79.85 3450 6.73 14.23 428 0 112.0 12/13/2022 14:24 80.07 3494 6.74 14.21 427 0 112.0 12/13/2022 14:25 80.29 3491 6.78 14.24 426 0 111.9 Pumping Rate Calculations [volume of water purged (gals) 80.29 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 370.00 [Final Depth to Water (feet) 71.20 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-mL Poly u None N Nitrate/nitrite as N y WATER 1 250-mL HDPE u H2SO4 (pH<2), 4 Deg C y Sulfate y WATER 1 250-mL HDPE u None N Total Dissolved Soilds y WATER 1 250-mL HDPE u 4 DegC y Heavy Metals -U only y WATER 1 250-mL HDPE y HN03 (pH<2) y Comments: [~rived on site at 0810. Purge began at 0815. Purged well for a total of 370 minutes. Purge ended and saml)_les collected at 1425. Water was clear. Left site at 1434. Signature of Field Technician -,. ' i .//~ / ---.)_. , 0 ,, ----·./·. -t/. _,,.-::<) Groundwater Discharge Permit .,....,.--:. Groundwater Monitoring Quality Assurance Plan White Mesa Mill ~-Field Data Worksheet For Groundwater Location ID MW-65 Sampling Program Field Sample ID MW-65 12132022 Sampling Event December Monthly Purge Date & Time Sample Date & Time 12/13/2022 12:25 [sampler TH/DL Purging Equipment Weather Conditions Pump Type External Ambient Temperature() Purging Method Previous Well Sampled Casing Volume () Calculated Casing Volumes Purge Duration () pH Buffer 7.0 Well Depth (ft) pH Buffer 4.0 Well Casing Diameter () Specific Conductance () Depth to Water Before Purging (ft) Date/Time Gallons Purg_ed Conductivi!¥_ pH Teme Redox [ Turbidity I Dissolved Oxygen I Before/After I Pumping Rate Calculations [volume of water purged() Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () [Final Depth to Water (feet) Number of casing Volumes Volume, if well evacuated to dryness () Name of Certified Analytical Laboratory Analytical Samples Information Container Preservative Type of Sample/ Analy_sis Sample Collected? Matrix Number Type Sample Filtered? T\fl)_e Added? Comments: [ Duplicate of MW-30 Signature of Field Technician -=-) ',·. •'-< --~-~ -!/--~-~ /-) TabD Quarterly Depth to Water Name: Tanner Holliday, Deen Lyman 11/17/2022 Depth to Depth to Depth to Water Date Time Well Water (ft.) Date Time Well Water (ft.) Date Time Well (ft.) 11/17/2022 1455 MW-01 65.08 11/17/2022 857 MW-04 82.35 11/17/2022 930 PIEZ-01 67.02 11/17/2022 1214 MW-02 109.65 I 1/17/2022 901 TW4-0l 101.06 I 1/17/2022 925 PIEZ-02 45.98 11/17/2022 1005 MW-OJA 83.90 11/17/2022 854 TW4-02 99,63 I\/\ 7/2022 801 PlEZ-03A 55.77 11 /17/2022 1229 MW-05 108,08 11 /17/2022 837 TW4-03 65,60 11/17/2022 1036 PIEZ-04 68.69 11/17/2022 1445 MW-II 85.33 11/17/2022 905 TW4-04 82.56 11/17/2022 1033 PlEZ-05 67.16 11/17/2022 1224 MW-12 109,53 11/17/2022 830 TW4-05 72.85 11/17/2022 742 TWN-01 70.16 11/17/2022 1312 MW-14 101.55 I 1/17/2022 911 TW4-06 80.20 11/17/2022 749 TWN-02 58.81 11/17/2022 1303 MW-15 105,27 11/17/2022 845 TW4-07 82.39 I 1/17/2022 753 TWN-03 43.80 11/17/2022 952 MW-17 72.18 11/17/2022 841 TW4-08 85.51 11/17/2022 757 TWN-04 62.85 11/17/2022 1436 MW-18 73.83 11/17/2022 827 TW4-09 70.93 11/17/2022 1432 TWN-06 80,68 11/17/2022 1427 MW-19 66.15 11/17/2022 824 TW4-IO 70.37 11/17/2022 1436 TWN-07 80.56 11/17/2022 1208 MW-20 89.27 11/17/2022 849 TW4-II 90.41 I 1/17/2022 1422 TWN-14 59.42 11/17/2022 1145 MW-22 66.35 11/17/2022 1013 TW4-12 56.55 I 1/17/2022 1417 TWN-16 47.84 11/17/2022 1220 MW-23 115.28 11/17/2022 1009 TW4-13 57.82 11/17/2022 805 TWN-18 62.96 11/17/2022 1147 MW-24A I 10.37 11/17/2022 1002 TW4-14 77 51 11/17/2022 1410 TWN-19 54.51 11/17/2022 1145 MW-24 109.21 11/17/2022 1027 TW4-16 74.39 11/17/2022 1445 TWN-20 78.18 11/17/2022 1433 MW-25 82.15 11/17/2022 739 TW4-18 74.06 11/17/2022 1448 TWN-21 79.18 11/17/2022 1438 MW-26 84.29 11/17/2022 1400 TW4-19 72.04 11/17/2022 1354 DR-05 83.15 11/17/2022 1141 MW-27 58.79 11/17/2022 735 TW4-21 72.25 11/17/2022 1349 DR-06 94.13 11/17/2022 1152 MW-28 74,60 11/17/2022 813 TW4-22 70.70 11/17/2022 1055 DR-07 91.72 11/17/2022 1155 MW-29 106.91 11/17/2022 919 TW4-23 76.79 11/17/2022 1342 DR-08 51.22 11/17/2022 1049 MW-30 75.51 11/17/2022 810 TW4-24 69.69 I 1/17/2022 1337 DR-09 86.55 11/17/2022 1044 MW-31 69,75 11/17/2022 745 TW4-25 69.95 11/17/2022 1333 DR-10 78.37 11/17/2022 1040 MW-32 82.93 11/17/2022 915 TW4-26 75.06 11/17/2022 1023 DR-II 97.88 11/17/2022 1246 MW-33 DRY 11/17/2022 934 TW4-27 79.45 11/17/2022 1016 DR-12 DRY I 1/17/2022 1254 MW-34 107.25 11/17/2022 1017 TW4-28 49.58 11/17/2022 IOI I DR-13 69,51 11/17/2022 1235 MW-35 1\2.35 11/17/2022 957 TW4-29 79.36 l l/17/2022 1323 DR-14 76.15 11/17/2022 1241 MW-36 110,52 11/17/2022 938 TW4-30 75.45 11/17/2022 1328 DR-15 92.81 11/17/2022 1301 MW-37 107.66 11/17/2022 941 TW4-31 76.43 11/17/2022 1318 DR-17 64,64 11/17/2022 1159 MW-38 70.13 11/17/2022 1020 TW4-32 57.32 11/17/2022 1304 DR-19 63,25 11/17/2022 1152 MW-39 64.39 11 /17/2022 931 TW4-33 79.08 11/17/2022 1300 DR-20 55.40 11/17/2022 944 MW-40 79.68 11/17/2022 949 TW4-34 77.67 11/17/2022 1221 DR-21 100.49 11/17/2022 953 TW4-35 75.98 11/17/2022 1309 DR-22 DRY MW-26 = TW4-15 11/17/2022 1006 TW4-36 58.87 11/17/2022 1255 DR-23 70.51 MW-32 = TW4-17 11/17/2022 816 TW4-37 7).95 I 1/17/2022 1313 DR-24 44.53 Comments: 11/17/2022 834 TW4-38 60.70 11/17/2022 820 TW4-39 70.60 11/17/2022 923 TW4-40 72.34 11/17/2022 908 TW4-41 89.17 11/17/2022 928 TW4-42 70,96 11/17/2022 945 TW4-43 73.64 TabE Laboratory Analytical Reports -Quarterly Sampling Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 L/,00~~\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-01_10192022 Matrix: Water Date Sampled: 10/19/22 10:10 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated lnor~anic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved 20.8 -3.7 19.4 I.OJ 1280 239 < 1.0 0.103 17.2 0.291 < 0.100 749 1300 < 0.0050 < 0.0005 < 0.0005 156 < 0.0250 <0.010 < 0.0100 0.35 < 0.0010 57.3 0.240 < 0.00050 < 0.0100 < 0.0200 6.3 < 0.0050 <0.010 153 < 0.0005 <0.10 < 0.0003 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 1.00 0.100 0.100 20.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10121122 10:57@ -0.9 ·c Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030 E SM 1030 E SM 2340 B SM2540 C SM 2320 B SM 2320 B EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1703 Preparation Date/Time 11/3/22 11/3/22 11/3/22 11/3/22 11/3/22 10/24/22 10/24/22 11/2/22 11/8/22 11/2/22 10/24/22 10/25/22 10/21/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/25/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 Lab ID: 22Jl 703-05 Analysis Date/Time 11/3/22 I 1/3/22 11/3/22 11/3/22 11/3/22 10/25/22 10/25/22 11/2/22 11/8/22 11/2/22 10/24/22 10/25/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 Page11of47 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORO Serving the lntermountain West Since 1953 LASOf;l,\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-01_10192022 (cont.) Matrix: Water Date Sampled: 10/19/22 10:10 Result ~lctals (rnnt.) Zinc, Dissolved < 0.0100 \'ohtlilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran 8.8 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1703 Preparation Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 Lab ID: 22Jl 703-05 Analysis Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 .fugfil Page 12 of 47 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 22, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: ----------Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-01_10192022 598057005 Ground Water 19-OCT-22 10:10 25-OCT-22 Client Parameter Qualifier Result Uncertain!r._ Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.234 The following Analytical Methods were performed: MDC 0.683 RL ----- 1.00 --------~--~-Method Descri tion --------------EPA 903.0 Project: Client ID: DNMIO0I00 DNMIO0l Units PF DF Analyst Date Time Batch Method pCi/L JXK3 11/20/22 1421 2339842 Anal st Comments Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 106 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 20 of 25 SDG: 598057 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L116OR,\T0RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-02_10202022 Matrix: Water Date Sampled: 10/20/22 9:10 Calcul.1tions Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated I nori.(anil' Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaCO3) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) i\lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 45.6 -0.6 45.1 1.00 3000 290 < 1.0 < 0.0500 6.57 0.221 <0.100 1910 3000 < 0.0050 < 0.0005 < 0.0005 320 < 0.0250 <0.010 < 0.0100 < 0.03 < 0.0010 93.2 < 0.0100 < 0.00050 < 0.0100 < 0.0200 10.2 0.0146 <0.010 487 < 0.0005 < 0.10 0.0112 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 1.00 0.100 0.100 50.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 5.0 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030£ SM 1030£ SM 1030 E SM 23408 SM2540C SM2320B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1703 Preparation Date/Time 11/3/22 11/3/22 I 1/3/22 11/3/22 11/3/22 10/24/22 10/24/22 11/2/22 I 0/31/22 11/2/22 10/25/22 10/26/22 10/21/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/25/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 Lab ID: 22Jl 703-09 Analysis Date/Time 11/3/22 11/3/22 11/3/22 11/3/22 11/3/22 10/25/22 10/25/22 11/2/22 11/2/22 11/2/22 10/25/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 fug{fil Page19of47 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH-FORD Serving the lntermountain West Since 1953 L/1801.:,\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-02_10202022 (cont.) Matrix: Water Date Sampled: 10/20/22 9:10 Result i\lctals (cont.) Zinc, Dissolved < 0.0100 \'olalilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22J1703 Preparation Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 Lab ID: 22Jl 703-09 Analysis Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 .E!..!!.g{fil Page 20 of 47 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 6, 2022 Parameter Company : Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-02 11012022 599611003 Ground Water 0l-NOV-22 09:55 04-NOV-22 Client Qualifier Result Uncertainty MDC RL Project: Client ID: DNMIO0l00 DNMIO0l Units PF DF Analyst Date Time Batch Method ----------- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha I .03 +/-0.292 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Test 0.645 1.00 pCi/L JXK3 I 1/20/22 1422 2339842 Anal st Comments Result Nominal Surrogate/Tracer Reco~~ Barium Carrier ----------------------Recovery% 114 Acceptable Limits (25%-125%) GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 17 of28 SDG: 599611 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Lt~80R~\TORIE5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-03A_10192022 Matrix: Water Date Sampled: 10/19/22 8:00 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated lnorganil· Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (IDS) ~lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved 80.7 -2.2 77.3 1.01 5240 294 < 1.0 < 0.0500 55.5 1.36 0.656 3520 5270 < 0.0050 < 0.0005 0.0007 426 < 0.0250 <0.010 < 0.0100 <0.03 < 0.0010 264 0.0486 < 0.00050 < 0.0100 < 0.0200 25.5 0.0975 < 0.010 773 < 0.0005 < 0.10 0.0180 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 20.0 0.500 0.100 50.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 5.0 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030E SM 1030 E SM 1030E SM2340B SM2540C SM2320B SM2320 B EPA 350.1 EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1703 Preparation Date/Time 11/3/22 11/3/22 I 1/3/22 11/3/22 11/3/22 10/24/22 10/24/22 11/2/22 10/25/22 11/2/22 10/24/22 11/8/22 10/21/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/25/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 Lab ID: 22Jl 703-06 Analysis Date/Time I 1/3/22 11/3/22 11/3/22 11/3/22 11/3/22 10/25/22 10/25/22 11/2/22 10/25/22 11/2/22 10/24/22 11/8/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 .E!.!fill. Page 13 of47 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 LA60R,\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-03A_10192022 (cont.) Matrix: Water Date Sampled: 10/19/22 8:00 i\lclals (cont.) Zinc, Dissolved 0.0142 \'olalilc Oq.(anic ( om pounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroforn1 < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1703 Preparation Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 Lab ID: 22Jl 703-06 Analysis Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 I 0/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 .E!J!.g_{fil Page 14 of 47 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 22, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW ----------Client Sample ID: MW-03A 10192022 Sample ID: 598057006 Matrix: Ground Water Collect Date: 19-OCT-22 08:00 Receive Date: 25-OCT-22 Collector: Client Parameter Qualifier Result Uncertainty MDC Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.253 0.747 The following Analytical Methods were performed: ----------Method Descri tion EPA 903.0 Surrogate/Tracer Recovery Test Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0I00 DNMIO0l Units PF DF Analyst Date Time Batch Method pCi/L JXK3 11/20/22 1421 2339842 Anal st Comments Result Nominal Recovery% Acceptable Limits I 07 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 21 of 25 SDG: 598057 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABOR o\ TOR IE S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-05_10122022 Matrix: Water Date Sampled: 10/12/22 14:15 Cakulalions Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnorganir Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated Total Dissolved Solids (TDS) \lcti1ls Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved 30.3 -1. 7 29.2 1.07 299 < 1.0 0.295 51.8 0.607 0.210 1100 1950 2080 < 0.0050 < 0.0005 < 0.0005 139 < 0.0250 < 0.010 < 0.0100 < 0.03 < 0.0010 39.7 0.105 < 0.00050 < 0.0100 < 0.0200 7.5 < 0.0050 < 0.010 433 < 0.0005 < 0.10 0.0004 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.00 0.100 0.100 JOO 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11:15@2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030 E SM I030 E SM2340B SM2320 B SM2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time 10/31/22 10/31/22 I 0/31/22 10/31/22 10/19/22 10/19/22 10/20/22 10/17/22 10/17/22 10/18/22 10/27/22 10/31 /22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21 /22 10/24/22 10/21/22 10/24/22 10/21/22 10/17/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Lab ID: 22J1153-07 Analysis Date/Time 10/31/22 10/31/22 10/31/22 10/31/22 10/19/22 10/19/22 10/27/22 10/17/22 10/17/22 10/18/22 10/28/22 10/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 I 0/21/22 10/21 /22 10/24/22 10/21/22 10/24/22 10/21/22 10/18/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21 /22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Page 15 of 53 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-05_10122022 (cont.) Matrix: Water Date Sampled: 10/12/22 14:15 :\lctals (cont.) Zinc, Dissolved < 0.0100 \'olatilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofonn < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran 2.2 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/14/22 11:15@2.1 ·c Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A CtF WO#: 22J1153 Preparation Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 Lab ID: 22J1153-07 Analysis Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 fuml Page 16 of 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 15, 2022 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-05 10122022 597226007 Ground Water 12-OCT-22 14:15 18-OCT-22 Client Qualifier Result Uncertainty ------------Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.173 The following Analytical Methods were performed: ---Method Description EPA 903.0 Surrogate/Tracer Recovery _J_es_t ____ _ MDC 0.652 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0l00 DNMIO0l Units PF DF Analyst Date Time Batch Method pCi/L LXB3 11/14/22 0801 2336187 Anal)'.St Commen=t=s __ _ Result Nominal Recovery% Acceptable Limits 97.5 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 20 of 29 SDG: 597226 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABOR>\TORlfS Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-11_10102022 Matrix: Water Date Sampled: 10/10/22 14:00 ( 'alrulations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnorg11nic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated Total Dissolved Solids (TDS) Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 31.2 3.7 33.6 1.23 271 < 1.0 0.365 72.1 0.231 2.90 1140 2090 2570 < 0.0050 < 0.0005 < 0.0005 150 < 0.0250 < 0.010 < 0.0100 <0.03 < 0.0010 51.0 0.214 < 0.00050 < 0.0100 < 0.0200 7.8 0.0155 <0.010 500 < 0.0005 <0.10 0.0024 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting !d!!.!l! 1.0 1.0 0.0500 1.00 0.100 0.100 100 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 5,0 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030 E SM2340 B SM2320B SM 2320 B EPA350.1 EPA300.0 EPA300.0 EPA 353.2 EPA300.0 SM2540 C SM 2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time 10/31/22 10/31/22 10/31/22 10/31/22 10/19/22 10/19/22 10/20/22 10/17/22 10/17/22 10/18/22 10/19/22 10/31/22 10/13/22 10/21 /22 10/21/22 10/21/22 10/24/22 10/21/22 10/21 /22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/17/22 10/21/22 10/21/22 10/24/22 10/21 /22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Lab ID: 22J1153-02 Analysis Date/Time 10/31/22 10/31/22 10/31/22 10/31/22 10/19/22 10/19/22 10/27/22 10/17/22 10/17/22 10/18/22 10/19/22 I 0/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21 /22 10/21 /22 10/24/22 10/21/22 10/24/22 10/21/22 10/18/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Page 5 of 53 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA60R,\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-11_10102022 (cont.) Matrix: Water Date Sampled: 10/10/22 14:00 Result \lclals (cont.) Zinc, Dissolved <0.0100 \ olatilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofom, < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/14/22 11:15@2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1153 Preparation Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 I 0/19/22 Lab ID: 22J1153-02 Analysis Date/Time 10/21/22 10/19/22 I 0/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 fug{fil Page 6 of 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 15, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW -----Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW-11 10102022 597226002 Ground Water 10-OCT-22 14:00 18-OCT-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.225 The following Analytical Methods were perfonned: Method Descri tion EPA 903.0 Surrogate/Tracer Recovery _T_e_s_t ____ _ MDC 0.599 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). Project: Client ID: DNMIO0I00 DNMIO0I RL Units PF DF Analyst Date Time Batch Method ---- 1.00 pCi/L LXB3 11/14/22 0803 2336187 -------'---'Anruyst Comments Result Nominal Recovery% Acceptable Limits 92.4 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 16 of 29 SDG: 597226 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA60R>\TOltlfS Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-12_10132022 Matrix: Water Date Sampled: 10/13/22 9:05 Cakulalions Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated Total Dissolved Solids (TDS) '.\lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 56.5 1.2 57.9 1.08 343 < 1.0 < 0.0500 67.0 0.130 0.149 2290 3630 3920 < 0.0050 < 0.0005 < 0.0005 513 < 0.0250 < 0.010 < 0.0100 <0.03 < 0.0010 228 0.0106 < 0.00050 < 0.0100 < 0.0200 13.5 0.0321 <0,010 304 < 0.0005 <0.10 0.0212 < 0.0 150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.00 0.100 0.100 100 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0,03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11:15@ 2.1 ·c Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030E SM 1030E SM 1030E SM2340 B SM 2320 B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2~40C SM 2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA 200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time 10/31/22 I 0/31/22 10/31/22 10/31/22 10/19/22 10/19/22 10/20/22 10/17/22 10/17/22 1 OIi 8/22 10/19/22 10/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/17/22 10/21/22 10/21/22 10/24/22 10/21 /22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Lab ID: 22J1153-11 Analysis Date/Time 10/31/22 10/31/22 10/31/22 10/31/22 10/19/22 10/19/22 10/27/22 10/17/22 10/17/22 10/18/22 10/20/22 10/31/22 10/17/22 I 0/21/22 I 0/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/18/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 .E!J!g{fil Page 23 of 53 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 LA60R>\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-12_10132022(cont.) Matrix: Water Date Sampled: 10/13/22 9:05 Result '\lrtals (ronl.) Zinc, Dissolved < 0.0I00 \"olalilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran 1.0 Toluene < 1.0 Xylenes, total < 1.0 'roject Name: 4th Quarter Ground Water 2022 rww. ChemtechFord. com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A CtF WO#: 22J1153 Preparation Date/Time 10/21/22 l0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 l0/19/22 l0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 Lab ID: 22J1153-11 Analysis Date/Time 10/21 /22 10/19/22 I 0/19/22 10/19/22 l0119/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 I 0/19/22 10/19/22 Flag(s) Page 24 of 53 = GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 15, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-12 10132022 597226011 Ground Water 13-OCT-22 09:05 18-OCT-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha u 1.00 +/-0.183 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.631 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0I00 DNMIO0I Units PF DF Analyst Date pCi/L LXB3 11/14/22 Anal st Comments Result Nominal Recovery% 96.7 Time Batch Method 1128 2336187 Acceptable Limits (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 24 of 29 SDG: 597226 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-14_10112022 Matrix: Water Date Sampled: 10/11/22 14:50 Cakulations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnor~anic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated Total Dissolved Solids (TDS) \lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 49.2 2.0 51.2 1.07 356 < 1.0 < 0.0500 18.4 <0.100 <0.100 2000 3200 3430 <0.0050 < 0.0005 0.0013 488 < 0.0250 <0.010 < 0.0100 <0.03 < 0.0010 154 1.73 < 0.00050 < 0.0100 < 0.0200 11.9 < 0.0050 <0.010 319 < 0.0005 < 0.10 0.0579 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.00 0.100 0.100 100 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 O.D3 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11: 15 @ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030 E SM 2340 B SM 2320 B SM 2320 B EPA350.I EPA300.0 EPA 300,0 EPA353.2 EPA300.0 SM2540C SM 2540 C EPA200.8 EPA 200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time 10/31/22 10/31/22 10/31/22 10/31/22 10/19/22 I 0/19/22 10/20/22 10/17/22 10/17/22 10/18/22 10/19/22 10/31/22 10/17/22 10/21/22 10/21 /22 10/21/22 10/24/22 10/21 /22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/17/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Lab ID: 22J1153-03 Analysis Date/Time 10/31/22 10/31 /22 10/31/22 10/31/22 10/19/22 10/19/22 10/27/22 10/17/22 10/17/22 10/18/22 10/19/22 10/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 I0/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/18/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 f!!g{fil Page 7 of 53 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Ll\80RATOl!IES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-14_10112022 (cont.) Matrix: Water Date Sampled: 10/11/22 14:50 \lctals (cont.) Zinc, Dissolved 0.0118 \ olatilc Oq~m1ic ( ·omroumts Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1153 Preparation Date/Time 10/21/22 I 0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 Lab ID: 22J1153-03 Analysis Date/Time 10/21/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 Page 8 of 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 15, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW ------- Client Sample ID: MW-14_10112022 Sample ID: 597226003 Matrix: Ground Water Collect Date: l l-OCT-22 14:50 Receive Date: 18-OCT-22 Collector: Client Parameter Qualifier Result Uncertainty MDC Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.174 0.771 The following Analytical Methods were performed: -------Method Descri tion RL 1.00 ---------------EPA 903.0 Surrogate/Tracer Recovery Test Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). Project: Client ID: DNMIO0l00 DNMIO0l Units PF DF Analyst Date Time Batch Method pCi/L LXB3 11/14/22 0801 2336187 ____ A_n_al __ _g_ Comments Result Nominal Recovery% Acceptable Limits IOI (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 17 of 29 SDG: 597226 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LMJOIIAfOll:l[S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-15_10122022 Matrix: Water Date Sampled: 10/12/22 10:30 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnor~anic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated Total Dissolved Solids (TDS) \I eta ls Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 49.7 6.1 56.2 I.II 337 < 1.0 < 0.0500 39.3 < 0.100 0.165 2010 3340 3720 < 0.0050 < 0.0005 < 0.0005 438 < 0.0250 <0.010 < 0.0100 < 0,03 < 0.0010 167 < 0.0100 < 0.00050 < 0.0100 < 0.0200 10.6 0.124 <0.010 467 < 0.0005 < 0.10 0.0422 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 I.OD 0.100 0.100 100 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 5.0 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11: 15 @ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030 E SM 2340 B SM 2320 B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540 C SM 2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time 10/3 1/22 10/31/22 I 0/31/22 10/31/22 10/19/22 10/19/22 10/20/22 10/17/22 10/17/22 10/18/22 10/19/22 10/31/22 10/17/22 10/21/22 10/21/22 I 0/21/22 10/24/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/17/22 10/21/22 I 0/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Lab ID: 22J1153-08 Analysis Date/Time 10/31/22 I 0/31/22 10/31/22 10/31/22 10/19/22 10/19/22 10/27/22 10/17/22 10/17/22 10/18/22 10/20/22 10/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21/22 10/24/22 I 0/21/22 10/24/22 10/21/22 10/18/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 fulill). Page 17 of 53 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA6ORAT0R1£S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-15_10122022 (cont.) Matrix: Water Date Sampled: 10/12/22 10:30 Result \lctals (cont.) Zinc, Dissolved < 0.0100 \'ulatilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofonn < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis Minimum Reporting Limit 0.0100 20.0 LO 1.0 1.0 1.0 20.0 LO LO 1.0 1.0 1.0 PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /503 0A EPA 8260D /5030A EPA 8260D 15030A CtF WO#: 22J1153 Preparation Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I Oil 9/22 10/19/22 I 0/19/22 10/19/22 10/19/22 Lab ID: 22J1153-08 Analysis Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 .El..!!Jilll Page 18 of 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 15, 2022 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW ----------Client Sample ID: MW-15 10122022 Sample ID: 597226008 Matrix: Ground Water Collect Date: 12-OCT-22 10:30 Receive Date: l 8-OCT-22 Collector: Client Project: Client ID: DNMIO0lO0 DNMIO0l Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method ----------------------'------------Parameter Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.319 0.881 1.00 pCi/L LXB3 I 1/14/22 0803 2336187 The following Analytical Methods were performed: Method Descri tion EPA 903.0 ----------------~A~n~a=-1 st Comments Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 69.9 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 21 of 29 SDG: 597226 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORAT0P.IES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-17_10172022 Matrix: Water Date Sampled: 10/17/22 11:00 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) Metals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 46.1 -1.5 44.7 1.05 2940 336 < 1.0 < 0.0500 54.0 0.224 1.11 1820 3090 < 0.0050 < 0.0005 < 0.0005 283 < 0.0250 < 0.010 < 0.0100 < 0.03 < 0.0010 140 0.0315 < 0.00050 < 0.0100 < 0.0200 9.8 0.0178 < 0.010 431 < 0.0005 <0.10 0.0195 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg.IL mg/L mg/L mg.IL mg.IL mg.IL mg.IL mg/L mg/L mg.IL mg.IL mg.IL mg.IL mg.IL mg.IL mg/L mg/L mg/L mg/L mg/L mg/L mg.IL mg/L mg/L mg/L mg/L mg.IL mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 20.0 0.100 0.100 20.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030 E SM2340 8 SM 2540 C SM 2320 8 SM2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1703 Preparation Date/Time 11/3/22 11 /3/22 11/3/22 11/3/22 11/3/22 10/24/22 10/24/22 11/2/22 10/25/22 11/2/22 10/24/22 10/25/22 10/21/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/25/22 10/26/22 10/26/22 10/24/22 10/26122 10126122 10/24/22 10/26122 10/24/22 10/26/22 10126/22 Lab ID: 22Jl 703-01 Analysis Date/Time 11/3/22 11/3/22 11/3/22 11/3/22 11/3/22 10/25/22 10/25/22 11/2/22 10/25/22 11/2/22 10/24/22 10/25/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 l0/24/22 10/26122 10/26/22 .E!.!!.w.l Page 3 of 47 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Ll\60RATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-17_10172022(cont.) Matrix: Water Date Sampled: 10/17/22 11:00 ~lctals (ront.) Zinc, Dissolved < 0.0100 \"olatilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofom1 < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www. Chem tech Ford. com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1703 Preparation Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 Lab ID: 22J1703-01 Analysis Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 .lli.lill}. Page 4 of 47 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 22, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-17 10172022 598057001 Ground Water l 7-OCT-22 11 :00 25-OCT-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.236 The following Analytical Methods were performed: MDC 0.909 RL 1.00 Project: Client ID: DNMIO0l00 DNMIO0l Units PF DF Analyst Date Time Batch Method pCi/L JXK3 11/20/22 1422 2339842 ----------------Method Descri tion Anal st Comments -------------~------~~ EPA 903.0 Surro_gate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 106 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 16 of 25 SDG: 598057 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/~BO~AT0A1£5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-18_10182022 Matrix: Water Date Sampled: 10/18/22 12:45 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated Inorganic Alkalinity• Bicarbonate (as CaC03) Alkalinity• Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) i\lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 49.7 -4.7 45.3 0.850 3100 345 < 1.0 < 0.0500 42.8 0.317 <0.100 2000 2640 < 0.0050 < 0.0005 < 0.0005 536 < 0.0250 < 0.010 < 0.0100 0.03 < 0.0010 126 0. 107 < 0.00050 < 0.0100 < 0.0200 7.6 < 0.0050 < 0.010 183 0.0020 <0.10 0.0246 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www. Chem tech Ford. com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 20.0 0.100 0.100 20.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/21/22 10:57@ -0.9 ·c Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday M£!h!ll! SM 1030 E SM 1030 E SM 1030 E SM2340 B SM2540C SM 2320B SM2320B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1703 Preparation Date/Time 11/3/22 11 /3/22 11/3/22 I 1/3/22 11/3/22 10/24/22 10/24/22 11/2/22 10/25/22 11/2/22 10/24/22 I 1/8/22 10/21/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/25/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 Lab ID: 22Jl 703-03 Analysis Date/Time 11/3/22 I 1/3/22 I 1/3/22 I 1/3/22 I 1/3/22 10/25/22 10/25/22 11/2/22 10/25/22 11/2/22 10/24/22 11/8/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 Page 7 of 47 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABOR,\TO RI ES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-18_10182022 (cont.) Matrix: Water Date Sampled: 10/18/22 12:45 Result :\lctals (cont.) Zinc, Dissolved < 0.0100 Volatile Organic Compounds Acetone <20.0 Benzene < LO Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday ~ EPA200.8 EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A CtF WO#: 22J1703 Preparation Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 Lab ID: 22Jl 703-03 Analysis Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 f!J!g{fil Page 8 of 47 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 22, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW ---Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW-18 10182022 598057003 Ground Water 18-OCT-22 12:45 25-OCT-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.203 The following Analytical Methods were performed: Method Descri tion ~---EPA 903.0 Test MDC 0.628 S~rrogate/Tracer Recovery Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). Project: DNMIO0 100 Client ID: DNMIO0 1 ----------RL Units PF 1.00 pCi/L JXK3 I 1/20/22 1422 2339842 ---------Anal)'.st Comm_!:nts __ Result Nominal Recovery% Acceptable Limit~ 109 (25%-125%) SRL = ample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows : DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration age 18 of 25 SDG: 598057 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit = I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD Serving the lntermountain West Since 1953 u~eoR~\TOJIIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-19_10172022 Matrix: Water Date Sampled: 10/17/22 14:25 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated Inorganic Alkalinity• Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) :\I eta ls Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 15.6 . 1.9 15.0 0.980 949 195 < 1.0 0.115 38.8 0.985 2.06 507 932 < 0.0050 < 0.0005 < 0.0005 132 <0.0250 <0.010 < 0.0100 < 0.03 < 0,0010 48.4 < 0.0100 < 0.00050 < 0.0100 < 0.0200 4.5 0.0139 < 0.010 98.4 < 0.0005 < 0.10 0.0062 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 20.0 0.200 0.100 20.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030E SM 1030E SM 2340 B SM2540 C SM2320 B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1703 Preparation Date/Time I 1/3/22 I 1/3/22 ll/3/22 11/3/22 I 1/3/22 10/24/22 10/24/22 11/2/22 10/25/22 11/2/22 10/24/22 10/25/22 10/21/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 I 0/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/25/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 Lab ID: 22Jl 703-02 Analysis Date/Time I 1/3/22 11/3/22 11/3/22 11/3/22 11/3/22 10/25/22 10/25/22 11/2/22 10/25/22 11/2/22 10/24/22 10/25/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 I 0/26/22 I 0/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 Page 5 of 47 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA60R,\TOAIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-19_10172022 (cont.) Matrix: Water Date Sampled: 10/17/22 14:25 Result \lctals (cont.) Zinc, Dissolved < 0.0100 \ olatile Organic Com pounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www. Chem tech Ford. com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /S030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /S030A EPA 8260D /S030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /S030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1703 Preparation Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 Lab ID: 22Jl 703-02 Analysis Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 ~ Page 6 of 47 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 22, 2022 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW --------------Client Sample ID: MW-19 10172022 Sample ID: 598057002 Matrix: Ground Water Collect Date: l 7-OCT-22 14:25 Receive Date: 25-OCT-22 Collector: Client Parameter Qualifier Result Uncertainty MDC ---------Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.272 0.676 The following Analytical Methods were perfonned: RL 1.00 Project: Client ID: DNMIO0l00 DNMIO0l Units PF DF Analyst Date Time Batch Method pCi/L JXK3 11/20/22 1422 2339842 Method Descri tion EPA 903.0 -----~------Anal)'st Comments Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 104 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 17 of25 SDG: 598057 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com Serving the lntermountain West Since 1953 CHEMTECH-FORD LA II ORATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-20_11012022 Matrix: Water Date Sampled: 11/1/22 12:00 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCOJ) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Result 67.3 -JO 54.9 1.08 4390 71.6 < 1.0 < 0.0500 60.8 0.202 7.12 3080 4740 < 0.0050 < 0.0005 < 0.0005 299 < 0.0250 <0.010 < O.OIOO < 0.03 < 0.0010 30.6 < 0.0100 < 0.00050 0.0159 < 0.0200 23.5 0.0062 < 0.010 848 < 0.0005 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Amended Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 1.00 0.100 2.00 50.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 5.0 0.0005 PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM I030 E SM 1030 E SM 1030 E SM2340 B SM 2540 C SM2320 B SM2320B EPA350.1 EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 CtF WO#: 22K0334 Preparation Date/Time 11/16/22 11/16/22 11/16/22 11/16/22 11/16/22 11/3/22 I 1/3/22 11/14/22 11/11 /22 11/11/22 I 1/8/22 11/18/22 11/4/22 11/14/22 11/14/22 I 1/14/22 I 1/8/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/8/22 11/14/22 11/10/22 11/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/8/22 11/14/22 Lab ID: 22K0334-03 Analysis Date/Time 11/28/22 I 1/28/22 11/28/22 11/28/22 11/28/22 11/3/22 11/3/22 11/14/22 11/14/22 11/14/22 11/8/22 I 1/19/22 11/4/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/8/22 11/14/22 11/10/22 11/14/22 11/14/22 11/8/22 11/14/22 11/14/22 I 1/8/22 11/14/22 Page 7 of 39 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD LABORATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-20_11012022 (cont.) Matrix: Water Date Sampled: 11/1/22 12:00 \lctals (cont.) Tin, Dissolved < 0.10 Uranium, Dissolved 0.0020 Vanadium, Dissolved < 0.0150 Zinc, Dissolved < 0.0100 \'olatilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofonn < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Amended Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.10 0.0003 0.0150 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22K0334 Preparation Date/Time 11/8/22 11/14/22 11/14/22 11/14/22 11/4/22 11/4/22 11 /4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 Lab ID: 22K0334-03 Analysis Date/Time 11/8/22 11/14/22 11/14/22 11/14/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 .E!.!!..Wl Page 8 of 39 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 6, 2022 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-20 11012022 599611004 Ground Water 0l-NOV-22 12:00 04-NOV-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.197 The following Analytical Methods were performed: MDC 0.585 RL 1.00 Project: Client ID: DNMIO0l00 DNMIO0l Units PF DF Analyst Date Time Batch Method pCi/L JXK3 11/20/22 1422 2339842 Method Descri tion EPA 903.0 __________________ A_n_a~l . _st Comments Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limit~ Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 111 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 18 of 28 SDG: 599611 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LAO:OtAfOIIIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-22_10192022 Matrix: Water Date Sampled: 10/19/22 13:20 ( "akulalions Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated lnor~anil· Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaC03) Ammonia asN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) '.\lclals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved V!anganese, Dissolved v1ercury, Dissolved v1olybdenum, Dissolved ~ickel, Dissolved 'otassium, Dissolved elenium, Dissolved ilver, Dissolved Jdium, Dissolved hallium, Dissolved n, Dissolved ·anium, Dissolved madium, Dissolved Result IOI -14 75.8 1.60 5920 < 1.0 < 1.0 1.08 53 .. 8 13.2 2.28 4780 9490 < 0.0050 0.0125 0.144 216 < 0.0250 0.453 0.106 0.04 0.0026 709 44.5 < 0.00050 0.393 0.261 10.5 0.0394 <0.010 148 0.0019 < 0.10 0.0200 <0.0150 oject Name: 4th Quarter Ground Water 2022 vw. ChemtechFord. com Certificate of Analysis -'1i!.. meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 20.0 0.500 0.100 100 50 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.0IO 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday SM I030 E SM 1030E SM 1030E SM 2340 B SM 2540 C SM 2320B SM2320B EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540 C EPA200.8 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA 200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1703 Preparation Date/Time I 1/3/22 11/3/22 11/3/22 I 1/3/22 11/3/22 10/24/22 10/24/22 I 1/2/22 10/25/22 I 1/2/22 10/24/22 10/26/22 l0/21/22 10/26/22 10/26/22 10/26/22 I 1/8/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 I 1/8/22 10/26/22 10/25/22 10/26/22 10/26/22 l 1/8/22 l0/26/22 10/26/22 I 1/8/22 10/26/22 10/24/22 10/26/22 10/26/22 Lab ID: 22Jl 703-07 Analysis Date/Time I 1/3/22 11/3/22 I 1/3/22 11/3/22 I 1/3/22 10/25/22 10/25/22 11/2/22 l 0/25/22 ll/2/22 10/24/22 10/26/22 10/24/22 10/26/22 I0/26/22 I0/26/22 I I/8/22 10/26/22 10/26/22 10/26/22 I0/24/22 10/26/22 I 1/8/22 10/26/22 I0/26/22 10/26/22 10/26/22 I 1/8/22 10/26/22 10/26/22 11/8/22 10/26/22 I0/24/22 10/26/22 10/26/22 Flag{s) Page 15 of 47 = Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LI.BOR,\TOAIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-22_10192022 (cont.) Matrix: Water Date Sampled: 10/19/22 13:20 Result ,\lclals (cont.) Zinc, Dissolved 1.12 \'olatilc Oq:;anic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone < 20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 LO 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A CtF WO#: 22J1703 Preparation Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 Lab ID: 22Jl 703-07 Analysis Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 .E!!lilll Page 16 of 47 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 22, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-22 10192022 598057007 Ground Water 19-OCT-22 13:20 25-OCT-22 Client Qualifier Result Uncertainty _________ ....;..__ Parameter Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 2.39 +/-0.448 The following Analytical Methods were performed: MDC 0.756 RL 1.00 Project: Client ID: DNMIO0I00 DNMIO0I Units PF DF Analyst Date Time Batch Method --- pCi/L JXK3 11/20/22 1422 2339842 -----------------Method Descri tion Anal st Comments _______ _ EPA 903.0 Surrogate/Tracer Recovery Test Result __ N_ominal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 94.8 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 22 of25 SDG: 598057 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD lA80RAt01UES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-23_11012022 Matrix: Water Date Sampled: 11/1/22 12:45 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \I eta ls Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Result 48.1 3.6 51.7 1.09 3210 254 < 1.0 < 0.0500 5.84 0.105 0.152 2060 3500 < 0.0050 < 0.0005 <0.0005 445 < 0.0250 <0.010 < 0.0100 < 0.03 < 0.0010 155 < 0.0100 < 0.00050 < 0.0100 < 0.0200 9.5 < 0.0050 <0.010 379 < 0.0005 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Amended Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 1.00 0.100 0.100 50.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0,010 0.5 0.0005 PO#: Receipt: 11/3/22 12:10@ -3.1 ·c Date Reported: 12/21/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030E SM 2340 B SM2540C SM 2320 B SM 23208 EPA350.I EPA300.0 EPA 300.0 EPA353.2 EPA300.0 SM 2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 CtF WO#: 22K0334 Preparation Date/Time 11/16/22 I 1/16/22 11/16/22 I 1/16/22 11/16/22 11/3/22 11/3/22 11/14/22 11/11/22 11/11/22 11/8/22 11/11/22 11/4/22 I 1/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/8/22 I 1/14/22 11/10/22 11/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/8/22 11/14/22 Lab ID: 22K0334-04 Analysis Date/Time 11/28/22 l l/28/22 11/28/22 11/28/22 1!/28/22 11/3/22 11/3/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/4/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/8/22 11/14/22 I 1/10/22 11/14/22 11/14/22 11/8/22 11/14/22 I 1/14/22 11/8/22 I 1/14/22 .E!.J!g{fil Page 9 of 39 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com Serving the lntermountain West Since 1953 CHEMTECH-FORD LABORATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-23_11012022 (cont.) Matrix: Water Date Sampled: 11/1/22 12:45 Result \lct.ils (cont.) Tin, Dissolved <0.10 Uranium, Dissolved 0.0071 Vanadium, Dissolved < 0.0150 Zinc, Dissolved < 0.0100 \'ol.itilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 11/3/22 12:10@-3.1 °C Date Reported: 12/21/2022 Amended Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.10 0.0003 0.0150 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22K0334 Preparation Date/Time 11/8/22 11/14/22 11/14/22 11/14/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 I 1/4/22 11/4/22 I 1/4/22 11/4/22 Lab ID: 22K0334-04 Analysis Date/Time 11/8/22 11/14/22 11/14/22 11/14/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 l 1/4/22 11/4/22 11/4/22 Page 10 of 39 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 6, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW -------------------------Client Sample ID: MW-23_11012022 Sample ID: 599611005 Matrix: Ground Water Collect Date: 01-NOV-22 12:45 Receive Date: 04-NOV-22 Collector: Client Qualifier Result Uncertainty -----------'-Parameter MDC RL Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U I.DO +/-0.285 0.727 I.OD The following Analytical Methods were performed: ------Method Descri lion EPA 903.0 Surrogate/Tracer Recovery Test Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). Project: Client ID: DNMIO0IO0 DNMIO0I Units PF OF Analyst Date Time Batch Method pCi/L JXK3 11/20/22 1422 2339842 Anal st Comments Result Nominal Recovery% Acceptable Limits I IO (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: OF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 19 of28 SDG: 599611 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com Serving the lntermountain West Since 1953 CHEMTECH·FORD !..ABORArORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample 10: MW-24_11022022 Matrix: Water Date Sampled: 11/2/22 6:45 ('akulalions Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaC03) Ammonia asN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) i\lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved 'Vlolybdenum, Dissolved '1ickel, Dissolved 'otassium, Dissolved ,elenium, Dissolved ;iJver, Dissolved ,odium, Dissolved 'halliurn, Dissolved 56.9 -10 46.4 1.23 3600 < 1.0 < 1.0 0.0691 44.1 1.53 0.325 2680 4440 < 0.0050 0.0033 0.0109 371 < 0.0250 0.134 0.0204 < 0.03 0.0027 155 8.13 < 0.00050 <0.0100 0.0869 JO.I 0.0184 <0.010 341 0.0035 ·roiect Name: 4th Quarter Ground Water 2022 ww. ChemtechFord.com Certificate of Analysis Amended Units meq/L % meq/L None rng/L mg/L mg/L mg/L mg/L rng/L mg/L mg/L mg/L rng/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 1.00 0.100 0.100 50.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.00IO 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030E SM 2340 B SM2540C SM2320 B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA 200.7 EPA200.8 CtF WO#: 22K0334 Preparation Date/Time 11/16/22 11/16/22 11/16/22 11/16/22 11/16/22 11/3/22 I 1/3/22 11/14/22 11/11/22 11/11/22 11/8/22 11/11/22 11/4/22 11/14/22 11/14/22 I 1/14/22 II/8/22 I 1/14/22 11/14/22 I 1/14/22 11/8/22 11/14/22 11/8/22 11/14/22 11/10/22 11/14/22 I 1/14/22 I 1/8/22 I 1/14/22 11/14/22 11/8/22 11/14/22 Lab ID: 22K0334-08 Analysis Date/Time 11/28/22 11/28/22 11/28/22 11/28/22 11/28/22 11/4/22 I 1/4/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/4/22 11/14/22 11/14/22 I 1/14/22 I 1/8/22 11/14/22 I 1/14/22 11/14/22 I 1/8/22 11/14/22 11/8/22 11/14/22 11/10/22 11/14/22 II/14/22 11/8/22 11/14/22 11/14/22 11/8/22 11/14/22 Page 17 of 39 = I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD LABORATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-24_11022022 (cont.) Matrix: Water Date Sampled: 11/2/22 6:45 Result \lctals (cont.) Tin, Dissolved < 0.10 Uranium, Dissolved 0.0075 Vanadium, Dissolved < 0.0150 Zinc, Dissolved 0.125 \'olatilc Organic Compoun<.ls Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Amended Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.10 0.0003 0.0150 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 8260D /5030A EPA 82600 /5030A EPA 8260D /503 0A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 8260D /5030A EPA 82600 /5030A CtF WO#: 22K0334 Preparation Date/Time 11/8/22 11/14/22 11/14/22 11/14/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 I 1/4/22 11/4/22 11/4/22 I 1/4/22 11/4/22 11/4/22 Lab ID: 22K0334-08 Analysis Date/Time 11/8/22 11/14/22 11/14/22 11/14/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 Page 18 of 39 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 6, 2022 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-24 11022022 599611011 Ground Water 02-NOV-22 06:45 04-NOV-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 2.70 +/-0.457 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.710 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0lO0 DNMIO0l Units PF DF Analyst Date Time Batch Method pCi/L JXK3 I 1/20/22 1422 2339842 Anal st Comments Result Nominal Recovery% Acceptable Limits 98.6 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 25 of28 SDG: 599611 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD LABOSIATOAIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-24A_11022022 Matrix: Water Date Sampled: 11/2/22 7:00 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated Inorganic Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaCO3) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Result 52.6 -8.2 44.6 1.27 3360 < 1.0 < 1.0 < 0.0500 44.3 1.86 0.266 2470 4260 < 0.0050 0.0050 0.0101 355 < 0.0250 0.136 0.0226 < 0.03 < 0.0010 145 7.13 < 0.00050 < 0.0100 0.0701 9.3 0.0193 <0.010 338 0.0029 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Amended Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 1.00 0.l00 0.100 50.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030E SM I030E SM 1030 E SM2340B SM 2540C SM2320 B SM2320 B EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 CtF WO#: 22K0334 Preparation Date/Time 11/16/22 11/16/22 11/16/22 11/16/22 11/16/22 I 1/3/22 IJ /3/22 I 1/14/22 11/11/22 I 1/11 /22 11/8/22 I 1/11/22 ll/4/22 11/14/22 11/14/22 IJ/14/22 11/8/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/8/22 11/14/22 IJ/10/22 11/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/8/22 I 1/14/22 Lab ID: 22K0334-09 Analysis Date/Time 11/28/22 ll/28/22 ll/28/22 11/28/22 I 1/28/22 11/4/22 11/4/22 11/14/22 ll/14/22 11/14/22 11/8122 11/14/22 11/4/22 11/14/22 I 1/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/14122 11/8/22 11/14/22 11/8/22 11/14/22 11/10/22 11/14/22 11/14/22 IJ/8/22 11/14/22 ll/14/22 11/8/22 11/14/22 .El.!!lilll Page 19 of 39 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD LABORA'r'ORll:S Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-24A_11022022 (cont.) Matrix: Water Date Sampled: 11/2/22 7:00 \lctals (cont.) Tin, Dissolved < 0.10 Uranium, Dissolved 0.0097 Vanadium, Dissolved < 0.0150 Zinc, Dissolved 0.0537 \'olatilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 11/3/22 12:10@ -3.1 ·c Date Reported: 12/21/2022 Amended Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.10 0.0003 0.0150 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22K0334 Preparation Date/Time 11/8/22 11/14/22 11/14/22 11/14/22 11/4/22 11/4/22 11/4/22 11/4/22 11 /4/22 11/4/22 11/4/22 11 /4/22 11/4/22 11/4/22 11/4/22 Lab ID: 22K0334-09 Analysis Date/Time 11/8/22 I 1/14/22 11/14/22 11/14/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 fugfil Page 20 of 39 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 6, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-24A 11022022 599611012 Ground Water 02-NOV-22 07:00 04-NOV-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 3.36 +/-0.458 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.531 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0I00 DNMIO0I Units PF DF Analyst Date Time Batch Method pCi/L JXK3 11/20/22 1422 2339842 Anal)'.st Comments Result Nominal Recovery% Acceptable Limits 111 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 26 of 28 SDG: 599611 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATOAIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-25_10102022 Matrix: Water Date Sampled: 10/10/22 10:40 Cakulatinns Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnor~anil· Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated Total Dissolved Solids (TDS) \ll'lals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 38.0 2.0 39.5 1.08 314 < 1.0 0.458 35.8 0.200 < 0.100 1480 2450 2660 < 0.0050 < 0.0005 0.0015 347 < 0.0250 0.010 < 0.0100 < 0.03 < 0.0010 123 1.36 < 0.00050 0.0166 < 0.0200 9.6 < 0.0050 <0.010 273 0.0009 <0.10 0.0064 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.00 0.100 0.100 100 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 O.Q3 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030 E SM2340 B SM 2320 B SM 2320 B EPA350.1 EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540 C SM2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200,8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time I 0/31/22 10/31/22 10/31/22 10/31/22 10/19/22 10/19/22 10/20/22 10/17/22 10/17/22 10/18/22 10/19/22 10/31/22 10/13/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/17/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Lab ID: 22J1153-01 Analysis Date/Time 10/31/22 10/31/22 10/31/22 10/31/22 10/19/22 10/19/22 10/27/22 10/17/22 10/17/22 I0/18/22 10/19/22 10/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/18/22 10/21/22 10/21/22 10/24/22 I0/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Page 3 of 53 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA80RATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-25_10102022 (cont.) Matrix: Water Date Sampled: 10/10/22 10:40 Result \ktals (rnnl.) Zinc, Dissolved < 0.0100 \ olatilc Organic ( 'om pounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofonn < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 PO#: Receipt: 10/14/22 11: 15 @ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D 15030A EPA 82600 /5030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1153 Preparation Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 Lab ID: 22J1153-01 Analysis Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 Page 4 of 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 15, 2022 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-25_10102022 597226001 Ground Water IO-OCT-22 10:40 18-OCT-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.189 MDC 0.763 RL 1.00 Project: Client ID: DNMIO0I00 DNMIO0I Units PF DF Analyst Date Time Batch Method pCi/L LXB3 11/14/22 0800 2336187 The following Analytical Methods were performed: ____ ___;::, _ __;;...._ ______ _:_ __________________ --- Method Descri tion EPA 903.0 Surrogate/Tracer Recovery _T_e_s_t _______ _ Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). Anal st Comments Result Nominal Recovery% Acceptable Limits 99.8 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 15 of 29 SDG: 597226 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LM!:OJ.:ATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-26_10132022 Matrix: Water Date Sampled: 10/13/22 8:45 ( 'alrulations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Ammonia as N Chloride Fluoride Nitrate + Nitrite, Total, as N Sulfate TDS, Calculated Total Dissolved Solids (TDS) \I dais Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 43.8 5.3 48.6 1.04 316 < 1.0 0.810 65.5 0.181 0.632 1710 2850 2970 <0.0050 < 0.0005 0.0006 526 < 0.0250 <0.010 < 0.0100 0.41 < 0.0010 178 0.972 < 0.00050 < 0.0IO0 < 0.0200 12.2 0.0063 < 0.010 171 < 0.0005 <0.10 0.0440 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.00 0.100 0.500 100 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0,5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11:15@ 2.1 ·c Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030 E SM 2340 B SM2320 B SM 2320 B EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540 C SM2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time I0/31/22 10/31/22 10/31/22 10/31/22 10/19/22 I0/19/22 10/20/22 10/17/22 10/17/22 10/18/22 10/19/22 10/31/22 10/17/22 10/21/22 I0/21/22 I 0/21/22 10/24/22 I0/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/17/22 10/21/22 I 0/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 I0/21/22 Lab ID: 22J1153-13 Analysis Date/Time 10/31 /22 10/31/22 I0/31 /22 I0/31/22 10/19/22 10/19/22 10/27/22 10/18/22 10/18/22 10/18/22 10/20/22 10/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 I0/21/22 10/21/22 10/24/22 10/21/22 10/24/22 I0/21/22 10/18/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 I 0/21 /22 10/24/22 10/21 /22 10/21/22 .El.!!lilll Page 27 of 53 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABOR:,, TO A lfS Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sam pie ID: MW-26_10132022 ( cont.) Matrix: Water Date Sampled: 10/13/22 8:45 Result \lctals (rnnl.) Zinc, Dissolved < 0.0100 \ olatilc Oq.:anir ( 0111po11111ls Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform 749 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis Minimum Reporting Limit 0.0100 20.0 1.0 1.0 100 1.0 20.0 1.0 1.0 1.0 1.0 1.0 PO#: Receipt: 10/14/22 11: 15 @ 2.1 ·c Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1153 Preparation Date/Time 10/21/22 I 0/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 I 0/19/22 10/19/22 Lab ID: 22J1153-13 Analysis Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 I 0/19/22 I 0/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 fug{fil Page 28 of 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 15, 2022 Parameter Company: Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW ------- MW-26 10132022 597226013 Ground Water 13-OCT-22 08:45 18-OCT-22 Client Qualifier Result Uncertainty MDC RL ------- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 1.50 +/-0.3 I 7 0.664 1.00 Project: Client ID: DNMIO0l00 DNMIO0I Units PF DF Analyst Date Time Batch Method pCi/L LXB3 I 1/14/22 I I 28 2336 I 87 The following Analytical Methods were performed: -=-----------~-----------Method Descri tion ________________ Anal stCornments EPA 903.0 Surrogate/Tracer Recovery Barium Carrier Notes: Test GFPC, Total Alpha Radium, Liquid "As Received" Counting Uncertainty is calculated at the 68% confidence level (I-sigma). Result Nominal Recovery% Acceptable Limits I I I (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 26 of 29 SDG: 597226 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA6QA:,\TOR1£S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-27_10192022 Matrix: Water Date Sampled: 10/19/22 14:30 Cakula1ior1, Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated lnoq!,artil· Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) AmmoniaasN Chloride Fluoride Nitrate + Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \lctal, Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved 13.9 -2.4 13.2 1.04 794 298 < 1.0 < 0.0500 30.7 0.722 5.26 334 828 < 0.0050 < 0.0005 < 0.0005 118 < 0.0250 <0.010 < 0.0100 <0.03 < 0.0010 47.8 < 0.0100 < 0.00050 <0.0100 < 0.0200 4.3 0.0148 <0.010 75.2 < 0.0005 < 0.10 0.0117 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 20.0 0.200 0.200 20.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/21/22 10:57@ -0.9 ·c Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030E SM 1030E SM 1030 E SM2340 B SM2540 C SM 2320 B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J 1703 Preparation Date/Time 11/3/22 11/3/22 11/3/22 I 1/3/22 11/3/22 10/24/22 10/24/22 I 1/2/22 10/25/22 I 1/2/22 10/25/22 10/25/22 10/21/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/25/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 Lab ID: 22Jl 703-08 Analysis Date/Time 11/3/22 11/3/22 11/3/22 11/3/22 11/3/22 10/25/22 10/25/22 11/2/22 10/25/22 11/2/22 10/25/22 10/25/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 .El.!!gW Page 17 of 47 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 u~aoR,\TO!JIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-27_10192022 (cont.) Matrix: Water Date Sampled: 10/19/22 14:30 Rcsull \lctals (cont.) Zinc, Dissolved < 0.0100 \'olalilc Organic ( 'om pounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/21/22 10:57@ -0.9 ·c Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday ~ EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J 1703 Preparation Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 I 0/26/22 10/26/22 10/26/22 10/26/22 10/26/22 Lab ID: 22Jl 703-08 Analysis Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 .E!.!gW Page 18 of 47 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analvsis Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-27 10192022 598057008 Ground Water 19-OCT-22 14:30 25-OCT-22 Client Parameter Qualifier Result Uncertainty MDC --'----- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.265 0.939 The following Analytical Methods were performed: RL 1.00 Project: Client ID: Report Date: November 22, 2022 DNMIO0I00 DNMIO0I Units PF DF Analyst Date Time Batch Method pCi/L JXK3 11/20/22 1422 2339842 Method Descri tion EPA 903.0 ---------~Anal st Comme~ _________ _ Surro~ate/Tracer Recovery'-_T_e_st_____ _ _______ R_es_u_lt ___ N_o_minal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 103 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 23 of25 SDG: 598057 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 L1,BOR1\T0l!IES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-28_10122022 Matrix: Water Date Sampled: 10/12/22 13:50 Cakulations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated Total Dissolved Solids (TDS) ~ lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 55.6 -0.2 55.3 0.990 162 < 1.0 < 0.0500 161 0.394 5.69 2290 3580 3550 0.0120 < 0.0005 0.0038 510 < 0.0250 0.024 < 0.0100 < 0.03 < 0.0010 195 1.04 < 0.00050 < 0.0100 0.0202 12.0 0.0237 <0.010 310 0.0009 < 0.10 0.0125 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 5.00 0.100 0.200 100 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0,00050 0.0100 0.0200 0.5 0.0050 0,010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030 E SM 1030E SM 2340 B SM2320B SM2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540 C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time 10/31/22 I0/31/22 10/31/22 10/31/22 10/19/22 10/19/22 10/20/22 10/19/22 10/17/22 10/18/22 10/27/22 I 0/31/22 10/17/22 10/21/22 10/21/22 10/21/22 I0/24/22 10/21/22 10/21/22 10/21/22 10/24/22 I 0/21/22 10/24/22 10/21/22 I 0/17/22 10/21/22 10/21/22 10/24/22 10/21 /22 10/21/22 10/24/22 10/21/22 10/24/22 I0/21/22 10/21/22 Lab ID: 22J1153-09 Analysis Date/Time I 0/31/22 10/31/22 10/31 /22 10/31/22 I 0/19/22 10/19/22 10/27/22 10/20/22 10/17/22 10/18/22 10/28/22 10/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21 /22 10/24/22 10/21/22 10/24/22 10/21/22 10/18/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21 /22 10/24/22 10/21/22 10/24/22 10/21/22 10/21 /22 fug{fil Page 19 of 53 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABO~AT0IIIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-28_10122022 (cont.) Matrix: Water Date Sampled: 10/12/22 13:50 Result l\lctals (cont.) Zinc, Dissolved 0.0396 \'olatilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 PO#: Receipt: 10/14/22 11: 15 @ 2.1 ·c Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A CtF WO#: 22J1153 Preparation Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 Lab ID: 22J1153-09 Analysis Date/Time I 0/21/22 10/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 Page 20 of 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company : Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Certificate of Analysis Energy Fuels Resources (USA}, Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-28_10122022 597226009 Ground Water 12-OCT-22 13:50 18-OCT-22 Client Project: Client ID: Report Date: November 15, 2022 DNMIO0l00 DNMIO0l Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method ---~----------"------------------Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.273 0.606 1.00 pCi/L LXB3 11/14/22 0803 2336187 The following Analytical Methods were performed: -----------------Method Descri tion -~----------------~An=a=I · _st Comments EPA 903.0 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 95.1 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 22 of 29 SDG: 597226 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy,UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA6OR>H0A1£S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-29_ 10122022 Matrix: Water Date Sampled: 10/12/22 9:55 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Inorganic Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated Total Dissolved Solids (TDS) '.\lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 52.3 8.8 62.4 1.16 298 < 1.0 0.654 38.4 0.481 <0.100 2180 3560 4130 0.0050 < 0.0005 < 0.0005 484 < 0.0250 < 0.010 < 0.0100 1.23 < 0.0010 225 5.06 < 0.00050 < 0.0100 < 0.0200 17.5 < 0.0050 <0.010 442 < 0.0005 < 0.10 0.0152 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www. Chem tech Ford. com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.00 0.100 0.100 100 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030E SM 1030 E SM 1030E SM 2340 B SM 2320 B SM2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time 10/31/22 I 0/31/22 I 0/31 /22 10/31/22 10/19/22 10/19/22 10/20/22 10/17/22 10/17/22 I 0/18/22 10/19/22 10/31/22 10/17/22 I 0/21/22 I 0/21 /22 10/21/22 10/24/22 I 0/21/22 I 0/21 /22 10/21 /22 10/24/22 10/21/22 10/24/22 10/21/22 10/17/22 10/21/22 10/21/22 10/24/22 10/21 /22 10/21 /22 10/24/22 10/21 /22 10/24/22 I 0/21/22 10/21/22 Lab ID: 22J1153-10 Analysis Date/Time 10/31/22 10/31/22 10/31/22 10/31/22 10/19/22 I 0/19/22 10/27/22 10/17/22 10/17/22 10/18/22 10/20/22 10/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 I 0/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/18/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 .El.!!Jilll Page 21 of 53 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD L"00ltil\T011E5" Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-29_10122022 (cont.) Matrix: Water Date Sampled: 10/12/22 9:55 Result :\!dais (cont.) Zinc, Dissolved < 0.0100 \ olatilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chlorofom1 < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/14/22 11:15@ 2.1 ·c Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1153 Preparation Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 Lab ID: 22J1153-10 Analysis Date/Time 10/21 /22 10/19/22 I 0/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 .E!..!!g{fil Page 22 of 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 15, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Contact: Lakewood, Colorado 80228 Ms. Kathy Weinel Project: White Mesa Mill GW ---Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW-29_10122022 597226010 Ground Water 12-OCT-22 09:55 18-OCT-22 Client --- Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.260 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Surrogate/Tracer Recovery Test MDC 0.754 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0l00 DNMIO0l Units PF DF Analyst Date Time Batch Method ---- pCi/L LX83 11/14/22 0803 2336187 Anal st Comments Result Nominal Re~ov~ry¾ Acceptable Limits -----------10 I (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 23 of 29 SDG: 597226 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-30_ 10132022 Matrix: Water Date Sampled: 10/13/22 10:10 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated Total Dissolved Solids (TDS) Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved ~ilver, Dissolved ,odium, Dissolved 'hallium, Dissolved "in, Dissolved Jranium, Dissolved 'anadium, Dissolved Result 23.0 3.8 24.8 1.22 156 < 1.0 < 0.0500 196 0.280 17.9 675 1450 1760 < 0.0050 < 0.0005 < 0.0005 281 < 0.0250 <0.010 < 0.0100 <0.03 < 0.0010 77.5 < 0.0100 < 0.00050 <0.0100 < 0.0200 6.8 0.0651 <0.010 98.3 < 0.0005 < 0.10 0.0098 < 0.0150 'roject Name: 4th Quarter Ground Water 2022 ww. ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 5.00 0.100 0.500 100 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030 E SM 23408 SM 2320 B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time 10/31/22 10/31/22 I 0/31/22 10/31/22 I 0/19/22 10/19/22 10/20/22 l0/19/22 10/17/22 l 0/18/22 10/19/22 10/31/22 10/18/22 10/21/22 l0/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/17/22 I 0/21/22 I 0/21/22 10/24/22 10/21/22 10/21/22 l0/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Lab ID: 22J1153-12 Analysis Date/Time 10/31/22 10/31/22 I 0/31/22 l 0/31/22 I 0/19/22 10/19/22 10/27/22 10/20/22 10/17/22 10/18/22 10/20/22 10/31/22 10/18/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/18/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 .E!.!!fill Page 25 of 53 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-30_10132022 (cont.) Matrix: Water Date Sampled: 10/13/22 10:10 :\lctals (cont.) Zinc, Dissolved < 0.0100 \"olatilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1153 Preparation Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 I 0/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 Lab ID: 22J1153-12 Analysis Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 Page 26 of 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 15, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-30_10132022 597226012 Ground Water 13-OCT-22 10:10 18-OCT-22 Client Qualifier Result Uncertainty -----Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.302 MDC 0.746 RL 1.00 Project: Client ID: DNMIO0I00 DNMIO0l Units PF OF Analyst Date Time Batch Method ---- pCi/L LX83 11/14/22 1128 2336187 The following Analytical Methods were performed: _c_ ________________ _ Method Description Anal st Comments -------------------~~~~~~~~----------EPA 903.0 Surrogate/Tracer Recovery __ Test __ _ _ ______ R_e_s_ul_t __ N_o_m_in_al Recove~% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 91.7 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 25 of 29 SDG: 597226 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-31_10112022 Matrix: Water Date Sampled: 10/11/22 13:10 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated Total Dissolved Solids (TDS) Metals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 35.5 6.9 40.8 1.23 191 < 1.0 < 0.0500 397 0.494 17.0 972 2220 2720 < 0.0050 < 0.0005 < 0.0005 391 < 0.0250 <0.010 < 0.0100 <0.03 < 0.0010 188 < 0.0100 < 0.00050 < 0.0100 < 0.0200 8.3 0.0973 < 0.010 128 < 0.0005 <0.10 0.0233 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 10.0 0.100 0.500 100 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11:15@ 2.1 ·c Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030 E SM2340 B SM 2320 B SM2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time 10/31/22 10/31/22 10/31/22 10/31/22 10/19/22 10/19/22 10/20/22 10/19/22 10/17/22 10/18/22 10/19/22 10/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/17/22 10/21/22 10/21/22 10/24/22 10/21/22 I 0/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Lab ID: 22J1153-04 Analysis Date/Time 10/31/22 10/31/22 10/31 /22 10/31/22 I 0/19/22 10/19/22 10/27/22 10/19/22 10/17/22 10/18/22 I 0/19/22 10/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/18/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 .E!J!g{fil Page 9 of 53 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-31_10112022 (cont.) Matrix: Water Date Sampled: 10/11/22 13:10 Result \letals (cont.) Zinc, Dissolved < 0.0100 \'ulatilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/14/22 11: 15 @ 2.1 ·c Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A CtF WO#: 22J1153 Preparation Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 Lab ID: 22J1153-04 Analysis Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 .El.!!.l:lll Page 10 of 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 15, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-31 10112022 597226004 Ground Water l l-OCT-22 13:10 18-OCT-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha I.II +/-0.315 The following Analytical Methods were performed: Method Descri tion EPA 903.0 SurrogateCf racer Recovery Test MDC 0.795 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0IO0 DNMIO0l Units PF DF Analyst Date pCi/L LXB3 11/14/22 Anal st Comments Result Nominal Recovery% 101 Time Batch Method 0803 2336187 Acceptable Limits (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 18 of 29 SDG: 597226 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABOR,\TOP.IES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-32_10112022 Matrix: Water Date Sampled: 10/11/22 11:45 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio Inorganic Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaC03) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated Total Dissolved Solids (TDS) \lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 48.4 2.8 51.2 1.07 354 < 1.0 0.603 37.1 0.133 < 0.100 1940 3120 3340 < 0.0050 < 0.0005 0.0015 494 < 0.0250 0.037 < 0.0100 5.15 < 0.0010 198 4.55 < 0.00050 0.0109 0.0461 13.8 < 0.0050 < 0.010 220 < 0.0005 <0.10 0.0019 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.00 0.100 0.100 100 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11:15@ 2.1 ·c Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030 E SM2340 B SM 2320 B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA 353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time 10/31/22 10/31/22 I 0/31/22 10/31/22 I 0/19/22 10/19/22 10/20/22 10/17/22 10/17/22 10/18/22 10/19/22 10/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/17/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Lab ID: 22J1153-05 Analysis Date/Time I 0/31/22 I 0/31/22 10/31/22 10/31/22 10/19/22 I 0/19/22 10/27/22 10/17/22 10/17/22 10/18/22 10/19/22 10/31/22 10/17/22 I 0/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21 /22 10/24/22 10/21/22 10/24/22 10/21/22 10/18/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Page 11 of 53 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABOR1\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-32_10112022 (cont.) Matrix: Water Date Sampled: 10/11/22 11 :45 i\lctals (root.) Zinc, Dissolved 0.0598 \'olatilc Organic Com rounds Acetone < 20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone < 20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D 15030A CtF WO#: 22J1153 Preparation Date/Time l 0/21 /22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 Lab ID: 22J1153-05 Analysis Date/Time 10/21/22 l 0/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 l 0/19/22 10/19/22 10/19/22 10/19/22 .E!J!gW Page 12 of 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 6, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter -- Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-32 10312022 599611002 Ground Water 31-OCT-22 13:00 04-NOV-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 1.85 +/-0.421 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Su1!_ogate/Tracer Recovery Test MDC 0.933 -Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: Units PF pCi/L DNMIO0l00 DNMIO0l DF Analyst Date JXK3 11/20/22 Anal st Comments Result Nominal Recovery% 110 Time Batch Method 1422 2339842 Acceptable Limits (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 16 of 28 SDG: 599611 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD lABOAATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-35_10312022 Matrix: Water Date Sampled: 10/31/22 13:45 ( alcuhltions Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Result 52.1 I.5 53.7 1.16 3400 305 < I.0 < 0.0500 60.6 0.305 <0.100 2130 3940 < 0.0050 < 0.0005 < 0.0005 496 < 0.0250 < 0.010 < 0.0100 0.21 < 0.0010 158 0.263 < 0.00050 < 0.0100 <0.0200 10.8 0.0121 <0.010 361 < 0.0005 Proiect Name: 4th Quarter Ground Water 2022 WWW. ChemtechFord. com Certificate of Analysis Amended Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 1.00 0.100 0.100 50.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 PO#: Receipt: 11/3/22 12:10@-3.1 °C Date Reported: 12/21/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030E SM 1030 E SM 1030E SM 2340 B SM2540C SM23208 SM 23208 EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 CtF WO#: 22K0334 Preparation Date/Time I 1/16/22 I I/I 6/22 I 1/16/22 JJ/16/22 I I/I 6/22 11/3/22 ll/3/22 I l/14/22 IJ/I 1/22 11/11/22 11 /8/22 11/I 1/22 11/4/22 11/14/22 11/14/22 11/14/22 11/8/22 ] J/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/8/22 11/14/22 11/J 0/22 I 1/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/8/22 11/14/22 Lab ID: 22K0334-0l Analysis Date/Time 11/28/22 11/28/22 1 I/28/22 11/28/22 I I/28/22 11/3/22 I 1/3/22 J J/14/22 I 1/14/22 11/14/22 11/8/22 I 1/14/22 1)/4/22 I 1/14/22 11/14/22 I 1/14/22 I I/8/22 J l/14/22 I l/14/22 JJ/14/22 JJ/8/22 11/14/22 11/8/22 11/14/22 I I/10/22 I 1/14/22 11/14/22 JJ/8/22 11/14/22 11/14/22 11/8/22 11/14/22 Flag(s) Page 3 of 39 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH·FORD LAROHAYO~IES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-35_10312022 (cont.) Matrix: Water Date Sampled: 10/31/22 13:45 i\lctals (cont.) Tin, Dissolved <0.10 Uranium, Dissolved 0.0223 Vanadium, Dissolved < 0.0150 Zinc, Dissolved < 0.0100 \'olatilc Or~anic Compounds Acetone < 20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/2112022 Amended Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.10 0.0003 0.0150 0.0100 20.0 1.0 1.0 1.0 1.0 20 0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22K0334 Preparation Date/Time 11/8/22 l l/14/22 l 1/14/22 11/14/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 Lab ID: 22K0334-01 Analysis Date/Time 11/8/22 l l/14/22 11/14/22 11/14/22 11/4/22 11/4/22 11 /4/22 I 1/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 Page 4 of 39 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 6, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW ---MW-35_10312022 599611001 Ground Water 31-OCT-22 13:45 04-NOV-22 Client Qualifier Result Uncertainty ----~--- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 3.26 +/-0.504 The following Analytical Methods were performed: MDC 0.819 RL 1.00 Project: Client ID: DNMIO0IO0 DNMIO0l Units PF DF Analyst Date Time Batch Method pCi/L JXK3 11/20/22 1422 2339842 ----------------------------------Method Descri tion ---~--------------------Anal st Comments EPA 903.0 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 106 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 15 of28 SDG: 599611 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 Ll,60RAT0RlfS Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-36_10112022 Matrix: Water Date Sampled: 10/11/22 14:35 Calculations Anions, Total Cation/Anion Balance Cations, Total IDS Ratio Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate IDS, Calculated Total Dissolved Solids (IDS) \lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 56.8 4.6 62.3 l.09 270 < l.0 < 0.0500 59.0 0.183 0.193 2390 3860 4210 < 0.0050 < 0.0005 < 0.0005 433 < 0.0250 <0.010 < 0.0100 <0.03 < 0.0010 140 < 0.0100 < 0.00050 < 0.0100 <0.0200 9.9 0.259 <0.010 665 0.0006 < 0.10 0.0220 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.00 0.100 0.100 100 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 5.0 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030E SM 1030E SM 2340 B SM 2320 B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200,8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time I 0/31/22 I 0/31/22 10/31 /22 10/31/22 10/19/22 10/19/22 10/20/22 10/17/22 10/17/22 10/18/22 10/19/22 10/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21 /22 10/24/22 10/21/22 10/24/22 10/21/22 10/17/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Lab ID: 22J1153-06 Analysis Date/Time I 0/31/22 I 0/31 /22 I 0/31/22 10/31/22 10/19/22 10/19/22 10/27/22 10/17/22 10/17/22 10/18/22 I 0/20/22 I 0/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21/22 10/24/22 I 0/21/22 10/24/22 10/21/22 10/18/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21 /22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 fug{fil Page 13 of 53 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD Serving the lntermountain West Since 1953 LA8Of;!,\T0RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-36_10112022 (cont.) Matrix: Water Date Sampled: 10/11/22 14:35 :\lctals (cont.) Zinc, Dissolved <0.0100 \'olatilc Or~anic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1153 Preparation Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 Lab ID: 22J1153-06 Analysis Date/Time 10/21/22 10/19/22 JO/I 9/22 I 0/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 .El.!!.rul Page 14 of 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 15, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW -------Client Sample ID: MW-36 10112022 Sample ID: 597226006 Matrix: Ground Water Collect Date: 11-OCT-22 14:35 Receive Date: 18-OCT-22 Collector: Client Parameter Qualifier Result Uncertainty MDC RL --=--------- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 1.00 +/-0.293 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Surrogate/Tracer Recovery Test ---- 0.723 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). 1.00 Project: Client ID: DNMIO0I00 DNMIO0I Units PF DF Analyst Date Time Batch Method pCi/L LXB3 11/14/22 0801 2336187 Anal st Comments Result Nominal Recovery% Acceptable Limits 99.4 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 19 of 29 SDG: 597226 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD LAl::ORA'rORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-37_11012022 Matrix: Water Date Sampled: 11/1/22 13:05 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) :\lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Result 52.2 3.1 55.5 1.13 3520 176 < 1.0 <0.0500 44.2 0.249 0.155 2280 4000 < 0.0050 < 0.0005 < 0.0005 466 < 0.0250 <0.010 < 0.0100 < 0.03 < 0.0010 132 0.0551 < 0.00050 < 0.0100 <0.0200 14.8 0.0085 <0.010 482 0.0008 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 1.00 0.100 0.100 50.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030E SM 1030 E SM 1030 E SM2340B SM 2540 C SM 2320 B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 CtF WO#: 22K0334 Preparation Date/Time 11/16/22 11/16/22 11/16/22 11/16/22 l 1/16/22 11/3/22 11/3/22 11/14/22 11/11/22 11/11/22 11/8/22 11/11/22 11/4/22 11/14/22 I l/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/14/22 11/8/22 I 1/14/22 I 1/8/22 11/14/22 I 1/10/22 11/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/8/22 11/14/22 Lab ID: 22K0334-05 Analysis Date/Time ll/28/22 11/28/22 ll/28/22 11/28/22 11/28/22 11/3/22 ] l/3/22 I 1/14/22 11/14/22 11/14/22 I 1/8/22 I 1/14/22 11/4/22 11/14/22 11/14/22 11/14/22 I 1/8/22 11/14/22 11/14/22 11/14/22 l 1/8/22 11/14/22 11/8/22 11/14/22 ll/10/22 11/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/8/22 11/14/22 Page 11 of 39 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD i.ABQ;iATO~IES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-37_11012022 (cont.) Matrix: Water Date Sampled: 11/1/22 13:05 Result \lctals (cont.) Tin, Dissolved < 0.10 Uranium, Dissolved 0.0120 Vanadium, Dissolved < 0.0150 Zinc, Dissolved 0.0232 \'olatilc Oqi;anic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Amended Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.10 0.0003 0.0150 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22K0334 Preparation Date/Time 11/8/22 11/14/22 11/14/22 11/14/22 11/4/22 11 /4/22 11 /4/22 11/4/22 11 /4/22 11 /4/22 11 /4/22 11/4/22 11 /4/22 11/4/22 11/4/22 Lab ID: 22K0334-05 Analysis Date/Time 11/8/22 11/14/22 11/14/22 11/14/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 I 1/4/22 11/4/22 f!..!!lill). Page 12 of 39 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 6, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW --------------- Client Sample ID: MW-37 11012022 Sample ID: 599611006 Matrix: Ground Water Collect Date: 0l-NOV-22 13:05 Receive Date: 04-NOV-22 Collector: Client Parameter Qualifier Result Uncertainty MDC Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.283 0.659 The following Analytical Methods were performed: RL 1.00 Project: Client ID: DNMIO0l00 DNMIO0I Units PF DF Analyst Date Time Batch Method pCi/L JXK3 11/20/22 1422 2339842 --------------------------------Method De::..:sc::.cr::..:i.c:..t::.io::..:n"-----------------------'-A=n=a,:e.1,_,sce.t--=C'-"o:..:..:m:.:..:m=en:.:..:t"'"s __________ _ EPA 903.0 Surrogate/Tra~r Recovery Test Nominal Recovery% Acceptable Limits -------Result Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" ! 03 (25%-I 25%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 20 of 28 SDG: 599611 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com Serving the lntermountain West Since 1953 CHEMTECH-FORD !.ABORATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-38_11012022 Matrix: Water Date Sampled: 11/1/22 12:30 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Result 49.8 6.0 56.1 l.15 3420 101 < 1.0 < 0.0500 40.3 1.37 14.8 2230 3930 < 0.0050 < 0.0005 < 0.0005 452 < 0.0250 <0.010 < 0.0100 <0.03 < 0.0010 183 < 0.0100 < 0.00050 < 0.0100 < 0.0200 26.4 0.178 <0.010 409 < 0.0005 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Amended Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 l.00 0.100 4.80 50.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030 E SM2340B SM 2540 C SM2320B SM2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 CtF WO#: 22K0334 Preparation Date/Time 11/16/22 11/16/22 11/16/22 11/16/22 11/16/22 11/3/22 11/3/22 11/14/22 11/11/22 11/11/22 11/8/22 11/11/22 11/4/22 11/14/22 ] ]/14/22 11/14/22 11/8/22 I 1/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/8/22 11/14/22 ]]/] 0/22 ll/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/8/22 11/14/22 Lab ID: 22K0334-06 Analysis Date/Time 11/28/22 11/28/22 l 1/28/22 11/28/22 11/28/22 11/3/22 11/3/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/4/22 11/14/22 11 /14/22 11/14/22 l l/8/22 11/14/22 11/14/22 l l/14/22 ll/8/22 11/14/22 11/8/22 ll/14/22 11/10/22 11/14/22 11/14/22 11/8/22 11/14/22 I 1/14/22 11/8/22 11/14/22 Page 13 of 39 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com Serving the lntermountain West Since 1953 CHEMTECH-FORD LA80RA'r0RIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-38_11012022 (cont.) Matrix: Water Date Sampled: 11/1/22 12:30 Result \lctals (cont.) Tin, Dissolved < 0.10 Uranium, Dissolved 0.0066 Vanadium, Dissolved <0.0150 Zinc, Dissolved < 0.0100 \'olatilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Proiect Name: 4th Quarter Ground Water 2022 www. Chem tech Ford. com Units mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Amended Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.10 0.0003 0.0150 0.0100 20.0 1.0 1.0 1.0 l.O 20.0 1.0 1.0 1.0 l.O 1.0 Sampled By: Tanner Holliday Method EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D 15030A EPA 8260D /5030A CtF WO#: 22K0334 Preparation Date/Time 11/8/22 11/14/22 11/14/22 11/14/22 11/4/22 11/4/22 l l/4/22 11/4/22 l 1/4/22 11/4/22 11/4/22 11/4/22 11/4/22 l l/4/22 11/4/22 Lab ID: 22K0334-06 Analysis Date/Time 11 /8/22 11/14/22 11/14/22 11/14/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 l J/4/22 11/4/22 Page 14 of 39 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 6, 2022 Parameter Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW ---------Client Sample ID: MW-38_11012022 Sample ID: 599611007 Matrix: Ground Water Collect Date: Ol-NOV-22 12:30 Receive Date: 04-NOV-22 Collector: Client Qualifier Result Uncertainty MDC RL Project: Client ID: DNMIO0I00 DNMIO0I Units PF DF Analyst Date Time Batch Method ---·------- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U LOO +/-0.206 0.566 LOO pCi/L JXK3 11/20/22 1422 2339842 The following Analytical Methods were performed: ---------------Method Description Analyst Comments EPA 903.0 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits --------- Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 106 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 21 of 28 SDG: 599611 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH-FORD Serving the lntermountain West Since 1953 lf1B0~1\TOP.IES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-39_10202022 Matrix: Water Date Sampled: 10/20/22 10:30 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated lnorganil· Alkalinity -Bicarbonate (as CaC03) Alkalinity -Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) I\Jctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved 63.6 -2.7 60.3 1.06 4200 < 1.0 < 1.0 0,214 37.4 0.647 <0.100 3010 4470 < 0.0050 0.0054 0.0025 418 < 0.0250 0.056 0.0208 13.2 < 0.0010 187 2.22 < 0.00050 < 0.0100 0.0297 13.9 0.0064 <0.010 527 0.0038 < 0.10 0.0098 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis !l.!!.i.!§ meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 20.0 0.200 0.100 50.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 5.0 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030E SM 1030 E SM 1030 E SM 2340 B SM2540C SM2320 B SM 2320 B EPA350.1 EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1703 Preparation Date/Time 11/3/22 I 1/3/22 I 1/3/22 I 1/3/22 Il/3/22 10/21/22 10/21/22 I 1/2/22 10/25/22 11/2/22 10/25/22 11/8/22 10/21/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/25/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 Lab ID: 22J1703-10 Analysis Date/Time 11/3/22 I 1/3/22 I 1/3/22 I 1/3/22 I 1/3/22 10/22/22 10/22/22 11/2/22 10/25/22 11/2/22 10/25/22 11/8/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 .E!J!ml Page 21 of 47 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD SeNing the lntermountain West Since 1953 LA60R,\TORIE5 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-39_10202022 (cont.) Matrix: Water Date Sampled: 10/20/22 10:30 Result ~lclals (rnnt.) Zinc, Dissolved 0.162 \'olalilc Or~anic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1703 Preparation Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 Lab ID: 22J1703-10 Analysis Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 Page 22 of 47 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 6, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-39 11012022 599611008 Ground Water 0l-NOV-2211:20 04-NOV-22 Client Qualifier Result Uncertainty ---Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 2.68 +/-0.454 The following Analytical Methods were performed: MDC 0.787 RL 1.00 Project: Client ID: DNMIO0I00 DNMIO0I Units PF DF Analyst Date Time Batch Method pCi/L JXK3 11/20/22 1422 2339842 --------------Method __ Des_gjption ------------------~A~n=al st Comments EPA 903.0 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 105 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (]-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 22 of 28 SDG: 599611 Rev 1 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LJ..BOR.\T0RIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-40_10182022 Matrix: Water Date Sampled: 10/18/22 11 :20 Cakulations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated Inorganic Alkalinity• Bicarbonate (as CaCO3) Alkalinity• Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) Metals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved Result 50.7 1.6 52.3 1.00 3310 228 < 1.0 < 0.0500 49.7 0.750 2.12 2150 3300 < 0.0050 < 0.0005 < 0.0005 447 < 0.0250 <0.010 < 0.0100 <O.D3 < 0.0010 192 0.0959 < 0.00050 < 0.0100 < 0.0200 8.7 0.217 <0.010 322 < 0.0005 <0.10 0.0216 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg.IL mg/L mg/L mg/L mg/L mg/L mg.IL mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 20.0 0.200 0.100 20.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030E SM 1030E SM 1030E SM2340 8 SM2540C SM23208 SM23208 EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1703 Preparation Date/Time 11/3/22 11/3/22 11/3/22 11 /3/22 11 /3/22 10/24/22 10/24/22 11/2/22 10/25/22 11/2/22 10/24/22 10/26/22 10/21/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/25/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 Lab ID: 22Jl 703-04 Analysis Date/Time 11/3/22 I 1/3/22 11/3/22 11/3/22 11/3/22 10/25/22 10/25/22 11/2/22 10/25/22 11/2/22 10/24/22 10/25/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 10/26/22 10/26/22 10/24/22 10/26/22 10/26/22 10/24/22 10/26/22 10/24/22 10/26/22 10/26/22 Page 9 of 47 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/,80~,\TORlfS Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-40_10182022 (cont.) Certificate of Analysis PO#: Receipt: 10/21/22 10:57@ -0.9 ·c Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Matrix: Water Lab ID: 22Jl 703-04 Date Sampled: 10/18/22 11 :20 Sampled By: Tanner Holliday Result ~lctals (cont.) Zinc, Dissolved < 0.0100 \'olatilc Org;inic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Minimum Reporting Preparation Limit Method Date/Time 0.0100 EPA200.8 10/26/22 20.0 EPA 8260D /5030A l 0/26/22 1.0 EPA 8260D /5030A 10/26/22 1.0 EPA 8260D /5030A 10/26/22 1.0 EPA 8260D /5030A 10/26/22 1.0 EPA 8260D /5030A 10/26/22 20.0 EPA 8260D /5030A 10/26/22 1.0 EPA 8260D /5030A l 0/26/22 1.0 EPA 8260D /5030A 10/26/22 1.0 EPA 8260D /5030A 10/26/22 1.0 EPA 8260D /5030A 10/26/22 1.0 EPA 8260D /5030A 10/26/22 CtF WO#: 22J1703 Analysis Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 .El.!!iltl Page 10 of 47 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 22, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW --------Client Sample ID: MW-40 10182022 Sample ID: 598057004 Matrix: Ground Water Collect Date: 18-OCT-22 11:20 Receive Date: 25-OCT-22 Collector: Client Parameter Qualifier Result Uncertainty MDC Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 1.04 +/-0.290 0.622 The following Analytical Methods were performed: Method Description EPA 903.0 Surrogate/Tracer Recovery Test Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0I00 DNMIO0I Units PF DF Analyst Date Time Batch Method pCi/L JXK3 11/20/22 1421 2339842 Anal st Comments Result Nominal Recove~% Acceptable Limits 110 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 19 of 25 SDG: 598057 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD LABORA't'O~IE.S Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: TW4-24_11012022 Matrix: Water Date Sampled: 11/1/22 13:30 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) AmmoniaasN Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \letnls Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved ~odium, Dissolved rhallium, Dissolved Result 104 4.8 114 1.06 6580 779 < 1.0 6.78 885 0.144 28.8 3010 6950 0.0055 < 0.0005 0.0010 604 < 0.0250 < 0.010 < 0.0100 < 0.03 < 0.0010 399 0.447 < 0.00050 0.918 0.0201 11.9 0.0855 <0.010 1170 0.0019 >roiect Name: 4th Quarter Ground Water 2022 vww. ChemtechFord. com Certificate of Analysis Amended Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.500 50.0 0.100 1.00 50.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 5.0 0.0005 PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday SM 1030 E SM 1030 E SM 1030 E SM 2340 B SM2540C SM2320 B SM 2320 B EPA350.1 EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.1 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 CtF WO#: 22K0334 Preparation Date/Time 11 /16/22 11/16/22 11/16/22 11/16/22 11/16/22 11/3/22 11 /3/22 11/14/22 11/11/22 11/11/22 11/8/22 11/11/22 11/4/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11 /14/22 1 l/14/22 11/8/22 11/14/22 I 1/8/22 11/14/22 11/10/22 11/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/8/22 11/14/22 Lab ID: 22K0334-07 Analysis Date/Time 11/28/22 l l/28/22 11/28/22 I 1/28/22 I 1/28/22 I 1/3/22 11/3/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/4/22 I 1/14/22 11/14/22 11/14/22 11 /8/22 11/14/22 11/14/22 11 /14/22 11/8/22 11 /14/22 11/8/22 11/14/22 11/10/22 11/14/22 11/14/22 11/8/22 11/14/22 I 1/14/22 11/8/22 11/14/22 Page 15 of 39 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD LABOaAYORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: TW4-24_11012022 (cont.) Matrix: Water Date Sampled: 11/1/22 13:30 Result :\lctals (cont.) Tin, Dissolved <0.10 Uranium, Dissolved 0.696 Vanadium, Dissolved < 0.0150 Zinc, Dissolved < 0.0100 \'olatilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform I 18 Chloromethane < 1.0 Methyl Ethyl Ketone < 20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran 4.4 Toluene < 1.0 Xylenes, total < 1.0 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported : 12/21/2022 Amended Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.10 0.0003 0.0150 0.0100 20.0 1.0 1.0 10.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A EPA 82600 /5030A CtF WO#: 22K0334 Preparation Date/Time 11 /8/22 11/14/22 11/14/22 11/14/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 Lab ID: 22K0334-07 Analysis Date/Time 11/8/22 11/14/22 11/14/22 11/14/22 11/4/22 I 1/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 ~ Page 16 of 39 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 6, 2022 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW TW4-24 11012022 599611010 Ground Water 0l-NOV-22 13:30 04-NOV-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.182 MDC 0.634 RL 1.00 The following Analytical Methods were performed: -'--------------- Project: Client ID: DNMIO0I00 DNMIO0I Units PF DF Analyst Date Time Batch Method pCi/L JXK3 11/20/22 1422 2339842 Method Descri"-t~io~n-'----------------------'Ac..=.cn=al'-'--=-st"-C=o1'-'-'11""111"'"e""n'""ts'-__ _ EPA 903.0 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits ------------ Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 114 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 24 of28 SDG: 599611 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 ll<.BO~ATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-65_10132022 Matrix: Water Date Sampled: 10/13/22 9:05 ( ·alrnl.ilions Anions, Total Cation/Anion Balance Cations, Total TDS Ratio lnor~anil· Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate TDS, Calculated Total Dissolved Solids (TDS) Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Tin, Dissolved Uranium, Dissolved Vanadium, Dissolved 56.6 0.7 57.4 1.08 344 < 1.0 0.620 67.0 < 0.100 0.137 2300 3630 3900 < 0.0050 < 0.0005 < 0,0005 509 < 0.0250 <0.010 < 0.0100 <0.03 < 0.0010 226 0.0106 < 0.00050 <0.0100 < 0.0200 13.4 0.0326 <0.010 302 < 0.0005 < 0.10 0.0212 < 0.0150 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Units meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 1.0 1.0 0.0500 1.00 0.100 0.100 100 5 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 0.10 0.0003 0.0150 PO#: Receipt: 10/14/22 11: 15 @ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030 E SM 2340 B SM 2320 B SM 2320 B EPA350.l EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540 C SM2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.l EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA200.8 CtF WO#: 22J1153 Preparation Date/Time 10/31/22 10/31/22 10/31 /22 10/31/22 10/19/22 I 0/19/22 10/20/22 10/17/22 I 0/1 7/22 I 0/18/22 10/19/22 10/31/22 10/17/22 10/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21/22 10/21/22 I0/24/22 10/21/22 10/24/22 10/21 /22 10/17/22 10/21/22 10/21 /22 10/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21/22 Lab ID: 22J1153-14 Analysis Date/Time 10/31/22 I0/31/22 10/31/22 10/31/22 10/19/22 10/19/22 10/27/22 10/18/22 10/18/22 I 0/18/22 10/20/22 10/31/22 10/17/22 I 0/21/22 10/21/22 10/21/22 10/24/22 10/21/22 10/21 /22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 I 0/18/22 I0/21/22 10/21/22 I0/24/22 10/21/22 10/21/22 10/24/22 10/21/22 10/24/22 10/21/22 10/21 /22 Page 29 of 53 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-65_10132022 (cont.) Matrix: Water Date Sampled: 10/13/22 9:05 Result \lclals (rnnt.) Zinc, Dissolved < 0.0100 \'olatik Oq.(anir ( 11111pm1111b Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com !l.!!.i.!§ mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1153 Preparation Date/Time 10/21/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 Lab ID: 22J1153-14 Analysis Date/Time 10/21/22 I0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I0/19/22 10/19/22 10/19/22 .E!.ruru1 Page 30 of 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 15, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-65 10132022 597226014 Ground Water 13-OCT-22 09:05 18-OCT-22 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha u 1.00 +/-0.293 The following Analytical Methods were performed: Method Descri tion EPA 903.0 Surrogate/Tracer Recove Test MDC 0.809 Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL 1.00 Project: Client ID: DNMIO0I00 DNMIO0I Units PF DF Analyst Date pCi/L LXB3 11/14/22 Anal st Comments Result Nominal Recovery% 96.7 Time Batch Method 1128 2336187 Acceptable Limits (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 27 of 29 SDG: 597226 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD lA80SfATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-70_10312022 Matrix: Water Date Sampled: 10/31/22 13:45 Calculations Anions, Total Cation/Anion Balance Cations, Total TDS Ratio TDS, Calculated Inorganic Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Ammonia as N Chloride Fluoride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \lctals Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Magnesium, Dissolved Manganese, Dissolved Mercury, Dissolved Molybdenum, Dissolved Nickel, Dissolved Potassium, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Thallium, Dissolved Result 52.9 2.2 55.3 1.10 3480 272 < 1.0 < 0.0500 67.2 0.245 <0.100 2190 3830 < 0.0050 < 0.0005 < 0.0005 512 < 0.0250 <0.010 < 0.0100 0.23 < 0,0010 163 0.203 < 0.00050 < 0.0100 < 0.0200 II.I 0.0128 <0.010 371 < 0.0005 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Certificate of Analysis Amended meq/L % meq/L None mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Minimum Reporting Limit 5 1.0 1.0 0.0500 1.00 0.100 0.100 50.0 20 0.0050 0.0005 0.0005 0.2 0.0250 0.010 0.0100 0.03 0.0010 0.2 0.0100 0.00050 0.0100 0.0200 0.5 0.0050 0.010 0.5 0.0005 PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Project Name: 4th Quarter Ground Water 2022 Sampled By: Tanner Holliday Method SM 1030 E SM 1030 E SM 1030 E SM2340B SM2540C SM2320B SM2320B EPA350.I EPA300.0 EPA300.0 EPA353.2 EPA300.0 SM 2540 C EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.7 EPA200.8 EPA245.I EPA200.8 EPA200.8 EPA200.7 EPA200.8 EPA200.8 EPA200.7 EPA200.8 CtF WO#: 22K0334 Preparation Date/Time 11/16/22 11/16/22 11/16/22 11/16/22 11/16/22 11/3/22 11/3/22 11/14/22 11/11/22 11/11 /22 11/8/22 11/11/22 11/4/22 11/14/22 11/14/22 11/14/22 11/8/22 I 1/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/8/22 11/14/22 11/10/22 11/14/22 I 1/14/22 11/8/22 11/14/22 11/14/22 11/8/22 I 1/14/22 Lab ID: 22K0334-02 Analysis Date/Time 11/28/22 11/28/22 11/28/22 11/28/22 11/28/22 11/3/22 11/3/22 11/14/22 11/14/22 11 /14/22 11 /8/22 11/14/22 11/4/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/14/22 11/8/22 11/14/22 11/8/22 11/14/22 11/10/22 11/14/22 11/14/22 11/8/22 11/14/22 11/14/22 11/8/22 11/14/22 Page 5 of 39 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD t.A80AAtOIUES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-70_10312022 (cont.) Matrix: Water Date Sampled: 10/31/22 13:45 \letals (cont.) Tin, Dissolved < 0.10 Uranium, Dissolved 0.0233 Vanadium, Dissolved < 0.0150 Zinc, Dissolved < 0.0100 \'olatilc Organic Compounds Acetone <20.0 Benzene < 1.0 Carbon Tetrachloride < 1.0 Chloroform < 1.0 Chloromethane < 1.0 Methyl Ethyl Ketone <20.0 Methylene Chloride < 1.0 Naphthalene < 1.0 Tetrahydrofuran < 1.0 Toluene < 1.0 Xylenes, total < 1.0 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Amended Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 0.10 0.0003 0.0150 0.0100 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA200.7 EPA200.8 EPA200.8 EPA200.8 EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 82600 /5030A EPA 8260D /5030A CtF WO#: 22K0334 Preparation Date/Time 11/8/22 I 1/14/22 11/14/22 11/14/22 I 1/4/22 11/4/22 I 1/4/22 11/4/22 I 1/4/22 I 1/4/22 11 /4/22 I 1/4/22 I 1/4/22 11/4/22 I 1/4/22 Lab ID: 22K0334-02 Analysis Date/Time 11/8/22 I 1/14/22 11/14/22 11/14/22 11/4/22 11/4/22 I 1/4/22 11 /4/22 I 1/4/22 11 /4/22 I 1/4/22 11/4/22 I 1/4/22 I 1/4/22 I 1/4/22 Page 6 of 39 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 6, 2022 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: -----------Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-70_10312022 599611009 Ground Water 31-OCT-22 13:45 04-NOV-22 Client Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 3.71 +/-0.514 The following Analytical Methods were performed: ---- MDC 0.721 RL Project: Client ID: DNMIO0I00 DNMIO0I Units PF DF Analyst Date Time Batch Method ------- 1.00 pCi/L JXK3 11/20/22 1422 2339842 Method Descri tion ________ _.c...A=n=a=I st Commen=t=s __ _ EPA 903.0 Surro~ate/Tracer Recovery Barium Carrier Notes: Test GFPC, Total Alpha Radium, Liquid "As Received" Counting Uncertainty is calculated at the 68% confidence level (I-sigma). Result Nominal Recovery% Acceptable Limits 111 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 23 of 28 SDG: 599611 Revl Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/,BORATOrnes Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 10/10/22 10:40 \"olatik Or:.:anil' ( ·om pounds Acetone Benzene Carbon Tetrachloride Chlorofonn Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total <20.0 < 1.0 < 1.0 < 1.0 < 1.0 <20.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA 8260D 15030A EPA 8260D 15030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1153 Preparation Date/Time 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 Lab ID: 22J1153-15 Analysis Date/Time 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 I 0/19/22 10/19/22 10/19/22 10/19/22 10/19/22 10/19/22 .lliJilll Page 31 of 53 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD Serving the lntermountain West Since 1953 Lt.60Ro\TORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 10/17/22 11:00 \ olatilc Org;mir Compounds Acetone Benzene Carbon Tetrachloride Chloroform Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total <20.0 < 1.0 < 1.0 < 1.0 < 1.0 <20.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Project Name: 4th Quarter Ground Water 2022 www. Chem tech Ford. com Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 10121122 10:57@ -0.9 ·c Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22J1703 Preparation Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 Lab ID : 22J1703-11 Analysis Date/Time 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 10/26/22 Page 23 of 47 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD LA808ATORIES Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 10/31/22 13:45 \'olatilc Organic Compounds Acetone Benzene Carbon Tetrachloride Chloroform Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total Result <20.0 < 1.0 < 1.0 < 1.0 < 1.0 <20.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Certificate of Analysis PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Amended Project Name: 4th Quarter Ground Water 2022 Minimum Reporting Limit 20.0 1.0 1.0 1.0 1.0 20.0 1.0 1.0 1.0 1.0 1.0 Sampled By: Tanner Holliday Method EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A EPA 8260D /5030A CtF WO#: 22K0334 Preparation Date/Time 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 Lab ID: 22K0334-10 Analysis Date/Time I 1/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 11/4/22 I 1/4/22 11/4/22 11/4/22 I 1/4/22 Page 21 of 39 9632 South 500 West I CHEMTECH·FORD LA80~ATORIES 11/1/2022 Work Order: 22J 1153 Project: 4th Quarter Ground Water 2022 Energy Fuels Resources, Inc. Attn: Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Client Service Contact: 801.262. 7299 The analyses presented on this report were performed in accordance with the National Environmental Laboratory Accreditation Program (NELAP) unless noted in the comments, flags, or case narrative. If the report is to be used for regulatory compliance, it should be presented in its entirety, and not be altered. Approved By: Melissa Connolly, Project Manager Sandy, Utah 84070 801.262.7299 Main 866.792.0093 Fax Serving the tntermountain West since 1953 www.ChemtechFord.com Page 1 of 53 CHEMTECH-FORD LABORATORIES Energy Fuels Resources, Inc. Project: 4th Quarter Ground Water 2022 Project Manager: Tanner Holliday Laboratory ID 22J1153-01 22J1153-02 22J1153-03 22J1153-04 22J1153-05 22J1153-06 22J1153-07 22J1153-08 22J1153-09 22J1153-10 22J1153-11 22J1153-12 22J1153-13 22J1153-14 22J1153-15 Sample Name MW-25_ 10102022 MW-11 _ 10102022 MW-14_10112022 MW-31_10112022 MW-32_ 10112022 MW-36_ 10112022 MW-05_ 10122022 MW-15_10122022 MW-28_10122022 MW-29_10122022 MW-12 _ 10132022 MW-30_ 10132022 MW-26_10132022 MW-65_10132022 Trip Blank Work Order Report Narrative Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions There are no corrective actions associated with this work order. Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 22J1153 Page 2 of 53 I CHEMTECH·FORD LABORAT0IIIES Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Certificate of Analysis Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations ND= Not detected at the corresponding Minimum Reporting Limit (MRL), PO#: Receipt: 10/14/22 11:15@ 2.1 °C Date Reported: 11/1/2022 Project Name: 4th Quarter Ground Water 2022 I mg/L = one milligram per liter or I mg/kg= one milligram per kilogram = I part per million I ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion. I ng/L = one nanogram per liter or I ng/kg = one nano gram per kilogram = 1 part per trillion. Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 22J1153 Page 32 of 53 3 American West Analytical Laboratories 463 W. 3600 S. Sall Lake City. UT 84115 Phone# (801) 263~686 Toll Free# (888) 263-1!686 .1-~ Fax# (801) 263~687 Email awal@awaHabs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 8. Hwy. 191 Blanding, UT 84511 Contact: TllDller Holliday Phone#: (435) 678-2221 Cell#: Email: tholllday@;eneqyfuela.com; KWelDe)@;enerr:,faela.com Project Name: 4th Quarter Ground Water 2022 Project#: PO#: Sampler Name: TllJlller Holliday ~S\\5°~ Samole ID: Date Samoled IIW-25_10102022 10/10/2022 IIW-l 1_10102022 10/10/2022 IIIW-14_10112022 10/11/2022 IIW-31_10112022 10/11/2022 · IIIW-32_10112022 10/11/2022 , IIW-36_10112022 10/11/2022 7 IIW-05_10122022 10/12/2022 8 IIW-15_10122022 10/12/2022 IIIW-28 10122022 10/12/2022 1 IIW-29_10122022 10/12/2022 IIW-12_10132022 10/13/2022 ' MW-30_10132022 -10/13/2022 ~Ollr,qulil,ed by: -~ JJ /~ L -ale: Slinn.ltu,o _..,_.. 10/1-.nn?? V t"una: Print Name: Tanner HolUdav 11nr IRolinqulohed by: 1)819: ls1anature Time: Prt,,tName: ~ollnqulahed by: Oate: Slanatun> Time: PrtnlName: Relinquished by: Dara: Slgnatunt [Time: PdntNsmc Time Samoled 1040 1400 1450 1310 1145 1435 1415 1030 1350 955 905 1010 ~-ed by. Sign.olUlo o.v.tNeme: R-.edby: Siglllllunl Print Noma: Received by: 51mu,1un, Print Name Rece1Vedby: SlnnAtun, PdntName: CHAIN OF CUSTODY Af1 analysis \MIi be conducted using NELAP accredited methods end all dale wHI be reported using AWAL'e standard analyte lists and reporting nmils (PQL) unless speciftcally requNled othenMt!.e on this Chain of Custody and/or attached documentation. AWAL Lab Sample Set# Page 1 of 2 I QC Level: I Tum Around Time: Unleas other anangements have been made, I""·"-oigned repo,1B w,11 be emaied by 5:00 pm on 3 Standard the day they are due. X Include EDD: Laboratory Use Only 0 LOCUS UPLOAD ::. <II EXCEL SanplaBWare: CJ .. .. X Field Filtered For. -:r: ::. Dmolvedlletala 1 Shipped o,hand-.....i -c II) ::. ~ '1-2 Arnbitm..-Chila! C'l .c i For Compliance Wrth: d-·\ ~ a. z □ NELAP 3 T-0 ,; c "C C [<, N □ RCRA o' C'l :i > D CWA .. R_,.,00 8--.g 0 ~ C 0 CJ ::i □ SOWA ~s-ed) -I') C 0 D ELAP/A2LA y N .., .. iii" c c::i ~ CJ □ NLLAP 0 0 en ~ II) 0 C'l -; .: □ Non-Compliance Sf',_iy-I') 0 I') CJ ¢ ~ .. II) ~ .. -a □ Other: y N 0 ~ .. .. IT f? !2. 0 IT = :a CJ .. Checkedalbalc:h )( ... < 0 ., 0 C Cl 10 y N C :E C'l 0 0 '1-Cl 'II ,; ,; ~ C'l ]i m 0 II) m ii u ID :::; II) .e en ~ Known Hazards 6 RecavedWtil C Ir: ~ ~ 0 .!! -u -!i .,; z 1111 • HoldingTmm u Q. N C'l ! = < g & "o E 0 e;! ;;" a y N .. .,i Ir: ... u iS 0 Sample Comments .. 7 w X X X X X X X X X X 7 w X X X X X X X X X X "-""TepeWa: 7 w X X X X X X X X X X 1 Prasant on Ou1w Padlage y N NA 7 w X X X X X X X X X X 2 -on Oular Padlage 7 w X X X X X X X X X X y N NA 7 w X X X X X X X X X X 3 "'-""Sample y N NA 7 w X X X X X X X X X X 4 -..onSarnple 7 w X X X X X X X X X X y N NA 7 w X X X X X X X X X X -Sample 7 w X X X X X X X X X X ~ Sid C0C ReCXJRI? y N 7 w X X X X X X X X X X 7 w X X X X X X X X X X ...,.;-/ -_.,;-';A:: ___,_ >; 0 f I I./ {.:,:;, Special Instructions: ----n1 '( IS- Sample containeTS for metals were field filtered. See the Date: Analytical Scope of Work for Reporting Limits and VOC analyte Time: list. Date: [Time; IOata: lrnne: Page 33 of 53 I American West Analytical Laboratories 463 W, 3600 S. Sall Lake City, UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 CHAIN OF CUSTODY All analyalo wtn be conducted using NELAP accn,a,ted melhodo and aA dala will be reported using AWAf.'s standard analyte lists and reporting limit& (POL) unless specifically requesled otherwise on this Chain of Cuatody and/or attached documentation. AWAI.. Lab Sample Set# Page 2 of 2 L --~ Fax# (801) 263-8687 Email awal@awal~abs.com I QC Level: I Tum Around Time: Unless-arrangements have lNNffl made, IDuc Oat~: I signed repor1B will be emailed by 5:00 pm on www.awal-labs.com 3 Standard lhedaylheyaredue. Client: Energy Fuels Resources, Inc. x Include EDD: l...aboratDry Use Only o LOCUS UPLOAD Address: 6425 8. Hwy. 191 ::e ~ EXCEL ~Wera: oii oii ~ Field Filtered For: Blanding, UT 84511 _ :i:: ::e Dlaolved Ketala 1 SNs>l>ed0t llao<l--.i --: i:: - Contact: Tanner Holliday ~ ::;, ~ 2 ,.,,_ ... a-~ t ~ For Compliance With: ~ \ Phone#: (435) 678-2221 Cell#:___________ ~ • i:: 0 NELAP 3 T--___ -c O & N □ RCRA Email: tholllda:,@energyfuela.com; KWelnel@:energyfuela.com ~ ~ -5 > 0 CWA 4 --.it.eaing 8 ~ CJ -□ SOWA ('-'15-edl Project Name: 4th Quarter Ground Water 2022 ~ c,:, ,..,, 8 0 ~ 0 ELAP I A2LA v N c::i ~ ~ ~ ~ t5 □NLLAP Project#: -----------------------------~ ::J 8 ~ -; U -□ Non-Compliance 5 "'-1f"'-val <'l ~ It) ~ ,.. -i:::: ,.._ 0 Other: Y N PO#:------------------------------fl ~ c, :t_ ll .a :S 8 oii o l5 "--------------,II Checkedatbench .,_~ o•olil _<o10 v N Tanner Holliday .s ;;; t') o O ~ o 11 ., .; 5 "' Sampler Name: ~ ::,; i ~ ~ ~ iii ,e: ~ rn ii ~ Known Hazards 6 Raceived Wllhin O G> ......_, ......_ --... -.. O D'J ·-CQ ■ Holdingilffl89 ~""\ ~ 3 Time u a. N t') u m .a II < z g & c::,f,ON,.J I ( S Samele ID: Date Sampled Sampled ~ l i ~ i: ~ ~ iS J > Samele Comments v " 1 IIW-26_10132022 10/13/2022 845 7 W X X X X X X X X X X 1 IIW-65 10132022 10/13/2022 905 7 W X X X X X X X X X X lr-rv-T-Waa: ; TRIPBLAKK 10/10/2022 1040 3 W X 1 ~-ana:-P~ NA ;l--------------------------l----------,lf-----f--+---,tl--f--t---11---11---11----,lf---i---i---i----i-------------t 2 U-m OulorP.,._ Y N NA r 3 Praoall on Sanple 1'-------------------------+----------11-----+-➔----11--+--+--1-----11-----11-----11-----1r----1r----1r-tr------------tl v N NA 11-------------------------+---------ll-----.f---l-----lt--t--+--t--l-----ll-----ll----11----lf----lf----,lf---------------il 4 U-a,anSanple Y N NA l l------------------~l----~I------I---IHl-+-+--+-l--+~l---+-~l---+----11-------------ilf----------i 1L ________________________ .J_ _____ _jl-____ J_-l-ll--l--l--l--l---l--ll---ll---ll---l~-1l-------------111'»~-~-s....,., ~,mCOCReconl? 1'-------------------------+----------11-----+-➔----11--+--+--1--1--1-----11-----1r----1r----1r-tr------------t1 v " ' L----------------------1------1------1-___,.---ll----ll--4-+--+--1---4--+-+--+----II------------II j .~ Rollnqwahodby; ~ /,J.// _/. .,,. ~oto: . ~~edby_:_.. .-, -..,,-,,r / ' 101•0 ~ _,,-, Special Instructions: Slonorur• -~--1 ""'Y 10/1312022 / / / ('( __,/ _,,.,, 'fl'-,/_.-"--------------------------1 .. pime: (../ ...... nm.. - 0 rlntName: TannerHolf,.._ 11nr Print Name: -, / / ..., Sample containers for metals were field filtered. See the Rollnqulahed by: Oale: Rece1va1 by; Date: Analytical Scope of Work for Reporting Limits and VOC analyte i.,....,•lllre Slgnalllre Time: nme: list. <>.int Name: Print Name: Retlnqutahed by: Oate: RecelVed by; Oale Signature Signabm, Time: Time· Pdnl N"""': Print Name: Rallnqutahed by; Date: Received by; Oale: Signature Sl!Jru,tu,e Time: jlme: 0 rin1Namo: Print Name: Page 34 of 53 Work Order# dd0 \\S3 Delivery Method: □ ups A Ps dEx o Chemtech Launer I I Courier ! ~ 821119 : I~ j l. "I! j (L' I i ~ E I .8 .. ' · ·--~.:;·.'-":: ~ ;: : , __ -_ ~LoU i:i .;: ]; .5 'o .,, l .~. 1 ~ Sample # Container . Preservative E J J .;_ o l-lt.{ -wl~') \ ;t_("\ ~ &\o \~\~ ~~ 1') \ )-.~;,). M \ \.%lo ,_ 'NL~J 'c a ]; 3! ~ Misc .5 l Volume (az/mll CHEMTECH FORD LABORATORIES Sample Receipt Receiving Temperature J.~ \ ·c ~ ~ ·--I ~ -· I -,. ,>j --.-I Comments ~ \~ ._,C> \o~ l\.lo \o~ CHEMTECH-FORD l/<BORATOP.l[S Sample Condition (check if yes I Sufficent Sample Volume Plastic Containers /\-Plutlc Unpre•or.-ed 8-Miscellaneous Plastic (. Cyanide Qt (NaOH) £ .. Colirorm/Ecoh/HPC f• Sulfide Qt (Zn Acetate) l• Mercury 1631 M· Metals Pint (HN03) N· Nutrient Pint (H2S04) R• Radiological (HN03) S· Sludge Cups/Tubs Q• Plastic Ba1 Glass Containers D-625 (Na25203) G-Gl.:ic;s Unpreserved H-HAAs (NH4CI) J-508/515/525 (Na2503) K-515.3 Herbicides 0-Oil & Grease (HCI) P-Phenols (H2504) T-TOC/TOX (H3P04) U-531 (MCAA, Na25203) V-524/THMs (Ascorbic Acid) W-8260VOC(Ll HCI) X-Vial Unpreserved Y-624/504 (Na25203) Z-Miscellaneous Glass Page 35 of 53 QC Report for Work Order (WO) -22J1153 Analyte % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -EPA 200.7 QC Sample ID: BWJI 118-BLKI Batch: BWJI 118 Date Prepared: I 0/24/2022 Date Analyzed: I 0/24/2022 Units: mg/L Calcium, Dissolved ND 0.2 1.00 Iron, Dissolved ND 0.03 1.00 Magnesium, Dissolved ND 0.2 1.00 Potassium, Dissolved ND 0.5 1.00 Sodium, Dissolved ND 0.5 1.00 Tin, Dissolved ND 0.10 1.00 LCS -EPA 200.7 QC Sample ID: 8 WJI I I 8-BS I Batch: BWJI I 18 Date Prepared: I 0/24/2022 Date Analyzed: I 0/24/2022 Units: mg/L Calcium, Dissolved 102 85 -115 10.4 10.2 0.2 1.00 Iron, Dissolved 103 85 -115 0.207 0.200 0.02 1.00 Magnesium, Dissolved 103 85 -115 10.5 10.2 0.2 1.00 Potassium, Dissolved 107 85 -115 10.7 10.0 0.5 1.00 Sodium, Dissolved 100 85 -115 10.0 10.0 0.5 1.00 Tin, Dissolved 93.9 85 -155 0.19 0.201 0.02 1.00 Matrix Spike -EPA 200.7 QC Sample ID: BWJI II8-MSI Batch: BWJI 118 QC Source Sample: 2211 I 53-0 I Date Prepared: I 0/24/2022 Date Analyzed: I 0/24/2022 Units: mg/L Calcium, Dissolved 91 .6 70 -130 356 347 10.2 0.2 1.00 Iron, Dissolved 97.3 70 -130 0.195 ND 0.200 0.02 1.00 Magnesium, Dissolved 106 70 -130 133 123 10.2 0.2 1.00 Potassium, Dissolved 110 70 -130 20.5 9.6 10.0 0.5 1.00 Sodium, Dissolved 90.6 70 -130 282 273 10.0 0.5 1.00 Tin, Dissolved 102 70 -130 0.20 ND 0.201 0.02 1.00 QC Sample ID: BWJI 118-MS2 Batch: BWJI 118 QC Source Sample: XXXXXXX-XX Date Prepared: I 0/24/2022 Date Analyzed: 10/24/2022 Units: mg/L Calcium, Dissolved 99.4 70 -130 54.7 44.5 10.2 0.2 1.00 Iron, Dissolved 101 70 -130 0.203 ND 0.200 0.02 1.00 Magnesium, Dissolved 102 70 -130 37.0 26.6 10.2 0.2 1.00 Potassium, Dissolved 108 70 -130 13.2 2.4 10.0 0.5 1.00 Sodium, Dissolved 93.7 70 -130 54.9 45.5 10.0 0.5 1.00 Tin, Dissolved 100 70 -130 0.20 ND 0.201 0.02 1.00 Matrix Spike Dup -EPA 200.7 QC Sample ID: BWJI 118-MSDl Batch: BWJI 118 QC Source Sample: 22JI I 53-0 I Date Prepared: 10/24/2022 Date Analyzed: I 0/24/2022 Units: mg/L Calcium, Dissolved 72.2 0.557 70 -130 20 354 347 10.2 0.2 1.00 Iron, Dissolved 100 3.14 70 -130 20 0.201 ND 0.200 0.02 1.00 Magnesium, Dissolved 99.9 0.441 70 -130 20 133 123 10.2 0.2 1.00 Potassium, Dissolved 111 0.818 70 -130 20 20.7 9.6 10.0 0.5 1.00 Sodium, Dissolved 71.5 0.677 70 -130 20 281 273 10.0 0.5 1.00 Tin, Dissolved 104 2.42 70 -130 20 0.21 ND 0.201 0.02 1.00 QC Sample ID: BWJI l l 8-MSD2 Batch: BWJI 118 QC Source Sample: XXXXXXX-XX Date Prepared: 10/24/2022 Date Analyzed: I 0/24/2022 Units: mg/L Calcium, Dissolved 101 0.233 70 -130 20 54.8 44.5 10.2 0.2 1.00 Iron, Dissolved 103 1.52 70-130 20 0.206 ND 0.200 0.02 1.00 Magnesium, Dissolved 103 0.204 70 -130 20 37.1 26.6 10.2 0.2 1.00 Potassium, Dissolved 107 0.723 70 -130 20 13.1 2.4 10.0 0.5 1.00 Sodium, Dissolved 94.3 0.108 70 -130 20 55.0 45.5 10.0 0.5 1.00 CtF WO#: 22J1153 www.ChemtechFord.com Page 36 of 53 Analyte QC Sample ID: BWJ1118-MSD2 Date Prepared: I 0/24/2022 Tin, Dissolved CtF WO#: 22J1153 www.ChemtechFord.com QC Report for Work Order (WO) -22J1153 %Rec RPO Limits RPO Max Result Source Cone Matrix Spike Dup -EPA 200.7 (cont.) Batch: BWJI 118 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/24/2022 Units: mg/L 101 0.494 70 -130 20 0.20 ND SpkValue MRL OF 0.201 0.02 1.00 Page 37 of 53 QC Report for Work Order (WO) -22J1153 Analyte %Rec RPD Limits RPDMax Result Source Cone SpkVa/ue MRL DF Blank -EPA 200.8 QC Sample ID: BWJI057-BLK1 Batch: BWJ1057 Date Prepared: 10/21/2022 Date Analyzed: 10/21/2022 Units: mg/L Arsenic, Dissolved ND 0.0050 1.00 Beryllium, Dissolved ND 0.0005 1.00 Cadmium, Dissolved ND 0.0005 1.00 Chromium, Dissolved ND 0.0250 1.00 Cobalt, Dissolved ND 0.010 1.00 Copper, Dissolved ND 0.0100 1.00 Lead, Dissolved ND 0.0010 1.00 Manganese, Dissolved ND 0.0100 1.00 Molybdenum, Dissolved ND 0.0100 1.00 Nickel, Dissolved ND 0.0200 1.00 Selenium, Dissolved ND 0.0050 1.00 Silver, Dissolved ND 0.010 1.00 Thallium, Dissolved ND 0.0005 1.00 Uranium, Dissolved ND 0.0003 1.00 Vanadium, Dissolved ND 0.0150 1.00 Zinc, Dissolved ND 0.0100 1.00 LCS -EPA 200.8 QC Sample ID: BWJ1057-BS1 Batch: BWJ1057 Date Prepared: 10/2 I /2022 Date Analyzed: 10/2 I /2022 Units: mg/L Arsenic, Dissolved 106 85 -115 0.042 0.0400 0.0005 1.00 Beryllium, Dissolved 102 85 -115 0.041 0.0400 0.0005 1.00 Cadmium, Dissolved 103 85 -115 0.041 0.0400 0.0002 1.00 Chromium, Dissolved 105 85 -115 0.042 0.0400 0.0005 1.00 Cobalt, Dissolved 104 85 -115 0.041 0.0400 0.0005 1.00 Copper, Dissolved 99.9 85 -115 0.040 0.0400 0.0010 1.00 Lead, Dissolved 105 85 -115 0.042 0.0400 0.0005 1.00 Manganese, Dissolved 103 85 -115 0.041 0.0400 0.0005 1.00 Molybdenum, Dissolved 106 85 -115 0.043 0.0400 0.0005 1.00 Nickel, Dissolved 101 85 -115 0.0404 0.D400 0.0005 1.00 Selenium, Dissolved 96.4 85 -115 0.039 0.0400 0.0005 1.00 Silver, Dissolved 105 85 -115 0.042 0.0400 0.0005 1.00 Thallium, Dissolved 113 85 -115 0.045 0.0400 0.0002 1.00 Uranium, Dissolved 98.8 85 -115 0.040 0.0400 0.0003 1.00 Vanadium, Dissolved 103 85 -115 0.041 0.0400 0.0005 1.00 Zinc, Dissolved 92.1 85 -115 0.037 0.0400 0.0100 1.00 Matrix Spike -EPA 200.8 QC Sample ID: BWJI057-MS1 Batch: BWJ1057 QC Source Sample: 2211153-01 Date Prepared: 10/21/2022 Date Analyzed: 10/2 I /2022 Units: mg/L Arsenic, Dissolved 112 70 -130 0.045 0.0003 0.0400 0.0005 1.00 Beryllium, Dissolved 103 70 -130 0.041 ND 0.0400 0.0005 1.00 Cadmium, Dissolved 96.4 70 -130 0.040 0.001 0.0400 0.0002 1.00 Chromium, Dissolved 97.9 70 -130 0.041 0.002 0.0400 0.0005 1.00 Cobalt, Dissolved 93.4 70 -130 0.047 0.010 0.0400 0.0005 1.00 Copper, Dissolved 87.2 70 -130 0.037 0.002 0.0400 0.0010 1.00 Lead, Dissolved 95.1 70 -130 0.038 ND 0.0400 0.0005 1.00 Manganese, Dissolved 112 70 -130 1.40 1.36 0.0400 0.0005 1.00 Molybdenum, Dissolved 107 70 -130 0.059 0.017 0.0400 0.0005 1.00 Nickel, Dissolved 89.3 75 -125 0.0444 0.0087 0.0400 0.0005 1.00 Selenium, Dissolved 115 70 -130 0.047 0.001 0.0400 0.0005 1.00 Silver, Dissolved 91 .8 70 -130 0.037 ND 0.0400 0.0005 1.00 CtF WO#: 22J1153 www.ChemtechFord.com Page 38 of 53 Ana/yte QC Sample ID: BWJ1057-MSI Date Prepared: I 0/2 I /2022 Thallium, Dissolved Uranium, Dissolved Vanadium, Dissolved Zinc, Dissolved QC Sample ID: BWJI057-MS2 Date Prepared: I 0/2 I /2022 Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Lead, Dissolved Manganese, Dissolved Molybdenum, Dissolved Nickel, Dissolved Selenium, Dissolved Silver, Dissolved Thallium, Dissolved Uranium, Dissolved Vanadium, Dissolved Zinc, Dissolved CtF WO#: 22J1153 www.ChemtechFord.com QC Report for Work Order (WO) -22J1153 %Rec RPO Limits RPDMax Result Source Cone Matrix Spike -EPA 200.8 (cont.) Batch: BWJ1057 QC Source Sample: 2211 I 53-0 I Date Analyzed: 10/21/2022 Units: mg/L 104 70 -130 0.043 0.0009 95.0 70 -130 0.044 0.006 98.8 70 -130 0.040 0.0006 115 70 -130 0.051 0.005 Batch: BWJ1057 QC Source Sample: XXXXXXX-XX Date Analyzed: I 0/2 I /2022 Units: mg/L 112 70 -130 0.045 0.0001 109 70 -130 0.044 ND 101 70 -130 0.040 ND 100 70 -130 0.042 0.002 98.4 70 -130 0.040 0.0002 92.2 70 -130 0.037 0.0003 99.8 70 -130 0.040 ND 100 70 -130 0.045 0.005 106 70 -130 0.043 0.001 94.7 75 -125 0.0392 0.0013 110 70 -130 0.046 0.002 99.9 70 -130 0.040 ND 108 70 -130 0.043 ND 96.1 70 -130 0.042 0.003 101 70 -130 0.041 0.0009 88.5 70 -130 0.037 0.001 SpkVa/ue MRL DF 0.0400 0.0002 1.00 0.0400 0.0003 1.00 0.0400 0.0005 1.00 0.0400 0.0100 1.00 0.0400 0.0005 1.00 0.0400 0.0005 1.00 0.0400 0.0002 1.00 0.0400 0.0005 1.00 0.0400 0.0005 1.00 0.0400 0.0010 1.00 0.0400 0.0005 1.00 0.0400 0.0005 1.00 0.0400 0.0005 1.00 0.0400 0.0005 1.00 0.0400 0.0005 1.00 0.0400 0.0005 1.00 0.0400 0.0002 1.00 0.0400 0.0003 1.00 0.0400 0.0005 1.00 0.0400 0.0100 1.00 Page 39 of 53 Analyte QC Sample ID: BWJ0785-BLK1 Date Prepared: 10/17/2022 Mercury, Dissolved QC Sample ID: BWJ0785-BSI Date Prepared: 10/17/2022 Mercury, Dissolved QC Sample ID: BWJ0785-MS1 Date Prepared: 10/17/2022 Mercury, Dissolved QC Sample ID: BWJ0785-MS2 Date Prepared: 10/17/2022 Mercury, Dissolved QC Sample ID: BWJ0785-MSDI Date Prepared: 10/17/2022 Mercury, Dissolved QC Sample ID: BWJ0785-MSD2 Date Prepared: 10/17/2022 Mercury, Dissolved CtF WO#: 22J1153 www.ChemtechFord.com QC Report for Work Order (WO) -22J1153 %Rec RPO Limits RPO Max Result Source Cone Blank -EPA 245.1 Batch: BWJ0785 Date Analyzed: 10/18/2022 Units: mg/L ND LCS -EPA 245.1 Batch: BWJ0785 Date Analyzed: I 0/18/2022 Units: mg/L 101 85 -115 0.00507 Matrix Spike -EPA 245.1 Batch: BWJ0785 QC Source Sample: 22J1153-01 Date Analyzed: 10/18/2022 Units: mg/L 94,3 75 -125 0.00472 ND Batch: BWJ0785 QC Source Sample: 2211153-02 Date Analyzed: 10/18/2022 Units: mg/L 98.6 75 -125 0.00493 ND Matrix Spike Dup -EPA 245.1 Batch: BWJ0785 QC Source Sample: 22J1153-01 Date Analyzed: 10/18/2022 Units: mg/L 97,7 3.56 75 -125 20 0.00489 ND Batch: BWJ0785 QC Source Sample: 2211153-02 Date Analyzed: 10/18/2022 Units: mg/L 96,8 1.78 75 -125 20 0.00484 ND SpkValue MRL OF 0.00050 1.00 0.00500 0.00015 1.00 0.00500 0.00015 1.00 0.00500 0.00015 1.00 0.00500 0.00015 1.00 0.00500 0.00015 1.00 Page 40 of 53 QC Report for Work Order (WO) -22J1153 Analyte %Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Blank -EPA 300.0 QC Sample ID: BWJ0796-BLK1 Batch: BWJ0796 Date Prepared: 10/17/2022 Date Analyzed: l 0/1 7 /2022 Units: mg/L Chloride ND 1.00 1.00 Fluoride ND 0.100 1.00 QC Sample ID: BWJ0807-BLK1 Batch: BWJ0807 Date Prepared: l 0/17 /2022 Date Analyzed: l 0/18/2022 Units: mg/L Chloride ND 1.00 1.00 Fluoride ND 0.100 1.00 QC Sample ID: BWJ0928-BLK1 Batch: BWJ0928 Date Prepared: l 0/19/2022 Date Analyzed: l 0/19/2022 Units: mg/L Chloride ND 1.00 1.00 Sulfate ND 1.00 1.00 QC Sample ID: BWJ0934-BLK1 Batch: BWJ0934 Date Prepared: 10/19/2022 Date Analyzed: 10/20/2022 Units: mg/L Chloride ND 1.00 1.00 Sulfate ND 1.00 1.00 QC Sample ID: BWJ0939-BLK1 Batch: BWJ0939 Date Prepared: 10/19/2022 Date Analyzed: l 0/20/2022 Units: mg/L Sulfate ND 1.00 1.00 QC Sample ID: BWJ1349-BLK1 Batch: BWJ1349 Date Prepared: 10/27/2022 Date Analyzed: l 0/28/2022 Units: mg/L Sulfate ND 1.00 1.00 LCS -EPA 300.0 QC Sample ID: BWJ0796-BS1 Batch: BWJ0796 Date Prepared: I 0/17 /2022 Date Analyzed: 10/17/2022 Units: mg/L Chloride 100 90 -110 50.0 50.0 1.00 1.00 Fluoride 102 90 -110 5.08 5.00 0.100 1.00 QC Sample ID: BWJ0807-BSI Batch: BWJ0807 Date Prepared: l 0/17 /2022 Date Analyzed: 10/18/2022 Units: mg/L Chloride 99.4 90 -110 49.7 50.0 1.00 1.00 Fluoride 103 90 -110 5.16 5.00 0.100 1.00 QC Sample ID: BWJ0928-BS l Batch: BWJ0928 Date Prepared: 10/19/2022 Date Analyzed: l 0/19/2022 Units: mg/L Chloride 99.7 90 -110 49.9 50.0 1.00 1.00 Sulfate 99.8 90 -110 49.9 50.0 1.00 1.00 QC Sample ID: BWJ0934-BS l Batch: BWJ0934 Date Prepared: l 0/19/2022 Date Analyzed: I 0/20/2022 Units: mg/L Chloride 99.9 90 -110 49.9 50.0 1.00 1.00 Sulfate 100 90 -110 50.1 50.0 1.00 1.00 QC Sample ID: BWJ0939-BS1 Batch: BWJ0939 Date Prepared: l 0/19/2022 Date Analyzed: l 0/20/2022 Units: mg/L Sulfate 100 90 -110 50.1 50.0 1.00 1.00 QC Sample ID: BWJ1349-BS1 Batch: BWJ1349 Date Prepared: 10/27/2022 Date Analyzed: l 0/28/2022 Units: mg/L Sulfate 100 90 -110 50.2 50.0 1.00 1.00 Matrix Spike -EPA 300.0 CtF WO#: 22J1153 www.ChemtechFord.com Page 41 of 53 QC Report for Work Order (WO) -22J1153 Analyte % Rec RPO Limits RPO Max Result Source Cone Matrix Spike -EPA 300.0 (cont.) QC Sample ID: BWJ0796-MSI Batch: BWJ0796 QC Source Sample: 2211153-0 I Date Prepared: I O/l 7 /2022 Date Analyzed: 10/17/2022 Units: mg/L Chloride 93.4 80 -120 46.2 35.8 Fluoride 75.3 80 -120 1.04 0.200 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recove!}'. of the LCS and the RPO. QC Sample ID: BWJ0796-MS2 Batch: BWJ0796 QC Source Sample: 2211153-02 Date Prepared: 10/17/2022 Date Analyzed: I 0/17 /2022 Units: mg/L Chloride 78.0 80 -120 80.8 72.1 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Fluoride 75.0 80 -120 1.06 0.231 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BWJ0807-MSI Batch: BWJ0807 QC Source Sample: XXXXXXX-XX Date Prepared: 10/17/2022 Date Analyzed: I 0/18/2022 Units: mg/L Chloride 140 80 -120 682 666 E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Fluoride 136 80 -120 2.32 0.806 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recove!}'. of the LCS and the RPO. QC Sample ID: BWJ0807-MS2 Batch: BWJ0807 QC Source Sample: XXXXXXX-XX Date Prepared: IO/I 7 /2022 Date Analyzed: I 0/18/2022 Units: mg/L Chloride 87.6 80 -120 687 677 Fluoride 96.4 80 -120 2.30 1.23 QC Sample ID: BWJ0928-MS1 Batch: BWJ0928 QC Source Sample: 2211153-01 Date Prepared: 10/19/2022 Date Analyzed: I 0/19/2022 Units: mg/L Chloride 91.3 80 -120 988 74.8 Sulfate 102 80 -120 2500 1480 QC Sample ID: BWJ0928-MS2 Batch: BWJ0928 QC Source Sample: XXXXXXX-XX Date Prepared: 10/19/2022 Date Analyzed: 10/19/2022 Units: Chloride 58.3 80 -120 494 435 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. Sulfate 94.0 80 -120 127 32.8 QC Sample ID: BWJ0934-MS1 Batch: BWJ0934 QC Source Sample: XXXXXXX-XX Date Prepared: 10/19/2022 Date Analyzed: 10/20/2022 Units: Chloride 93.9 80 -120 114 19.8 Sulfate 90.2 80 -120 90.2 ND QC Sample ID: BWJ0934-MS2 Batch: BWJ0934 QC Source Sample: XXXXXXX-XX Date Prepared: 10/19/2022 Date Analyzed: 10/20/2022 Units: Chloride 77.2 80 -120 712 634 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. CtF WO#: 22J1153 www.ChemtechFord.com mg/L mg/L mg/L Spk Value MRL OF 11.1 1.11 1.00 1.11 0.111 1.00 11.1 1.11 1.00 1.11 0.111 1.00 11.1 1.11 1.00 1.11 0.111 1.00 11.1 1.11 1.00 1.11 0.111 1.00 1000 110 1.00 1000 110 1.00 100 11 .0 1.00 100 11 .0 1.00 100 11.0 1.00 100 11.0 1.00 100 11.0 1.00 Page 42 of 53 Analyte QC Sample ID: BWJ0934-MS2 Date Prepared: I 0/19/2022 Sulfate QC Sample ID: BWJ0939-MSI Date Prepared: 10/19/2022 Sulfate QC Sample ID: BWJ0939-MS2 Date Prepared: I 0/l 9/2022 Sulfate QC Sample ID: BWJ1349-MS1 Date Prepared: 10/27/2022 Sulfate QC Sample ID: BWJ1349-MS2 Date Prepared: 10/27/2022 Sulfate QC Report for Work Order (WO) -22J1153 % Rec RPD Limits RPD Max Result Source Cone Matrix Spike -EPA 300.0 (cont.) Batch: BWJ0934 QC Source Sample: XXXXXXX-XX Date Analyzed: I 0/20/2022 Units: mg/L 88.0 80 -120 173 85.4 Batch: BWJ0939 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/20/2022 Units: mg/L 92.9 80 -120 10.3 ND Batch: BWJ0939 QC Source Sample: XXXXXXX-XX Date Analyzed: I 0/20/2022 Units: mg/L 105 80 -120 58,7 47.1 Batch: BWJ1349 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/28/2022 Units: mg/L 107 80-120 63.0 51.2 Batch: BWJ1349 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/28/2022 Units: mg/L 24.6 80-120 1550 1540 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWJ0796-MSDI Date Prepared: 10/17/2022 Chloride Fluoride Matrix Spike Dup -EPA 300.0 Batch: BWJ0796 QC Source Sample: 22Jll53-0l Date Analyzed: 10/17/2022 Units: mg/L 93.6 0.0303 80 -120 20 46.2 35.8 75.2 0.172 80 -120 20 1.03 0.200 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BWJ0796-MSD2 Date Prepared: 10/l 7 /2022 Chloride Fluoride Batch: BWJ0796 QC Source Sample: 2211153-02 Date Analyzed: 10/17/2022 Units: mg/L 87.7 1.32 80 -120 20 81.8 72.1 76,2 1.29 80-120 20 1.08 0.231 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BWJ0807-MSD1 Date Prepared: 10/17/2022 Chloride Batch: BWJ0807 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/18/2022 Units: mg/L 130 0.160 80 -120 20 681 666 E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Fluoride 128 3.80 80 -120 20 2.23 0.806 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BWJ0807-MSD2 Date Prepared: 10/17/2022 Chloride Fluoride QC Sample ID: BWJ0928-MSD1 Date Prepared: 10/19/2022 Chloride CtF WO#: 22J1153 www.ChemtechFord.com Batch: BWJ0807 QC Source Sample: XXXXXXX-XX Date Analyzed: I 0/18/2022 85.0 102 0.0425 2.74 80 -120 80 -120 20 20 687 2.36 Units: mg/L 677 1.23 Batch: BWJ0928 QC Source Sample: 22Jl 153-0 I Date Analyzed: 10/19/2022 91.1 0.173 80 -120 20 986 Units: mg/L 74.8 Spk Value 100 11.1 11.1 11.1 50.0 11.1 1.11 11.1 1.11 11.1 1.11 11.1 1.11 1000 MRL 11.0 1.11 1.11 1.11 5.50 1.11 0.111 1.11 0.111 1.11 0.111 1.11 0.111 110 DF 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 Page 43 of 53 QC Report for Work Order (WO) -22J1153 Analyte % Rec RPD Limits RPO Max Result Source Cone Matrix Spike Dup -EPA 300.0 (cont.) QC Sample ID: BWJ0928-MSD1 Batch: BWJ0928 QC Source Sample: 2211153-01 Date Prepared: 10/19/2022 Date Analyzed: 10/19/2022 Units: mg/L Sulfate 102 0.152 80 -120 20 2490 1480 QC Sample ID: BWJ0928-MSD2 Batch: BWJ0928 QC Source Sample: XXXXXXX-XX Date Prepared: 10/19/2022 Date Analyzed: 10/19/2022 Units: mg/L Chloride 59.0 0.138 80 -120 20 494 435 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. Sulfate 92.3 1.38 80 -120 20 125 32.8 QC Sample ID: BWJ0934-MSDI Batch: BWJ0934 QC Source Sample: XXXXXXX-XX Date Prepared: 10/19/2022 Date Analyzed: I 0/20/2022 Units: mg/L Chloride 93.4 0.416 80 -120 20 113 19.8 Sulfate 89.8 0.487 80 -120 20 89.8 ND QC Sample ID: BWJ0934-MSD2 Batch: BWJ0934 QC Source Sample: XXXXXXX-XX Date Prepared: 10/19/2022 Date Analyzed: 10/20/2022 Units: mg/L Chloride 73.3 0.548 80 -120 20 708 634 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Sulfate 88.0 0.00443 80 -120 20 173 85.4 QC Sample ID: BWJ0939-MSDI Batch: BWJ0939 QC Source Sample: XXXXXXX-XX Date Prepared: 10/19/2022 Date Analyzed: I 0/20/2022 Units: mg/L Sulfate 93.4 0.462 80 -120 20 10.4 ND QC Sample ID: BWJ0939-MSD2 Batch: BWJ0939 QC Source Sample: XXXXXXX-XX Date Prepared: 10/19/2022 Date Analyzed: 10/20/2022 Units: mg/L Sulfate 105 0.0789 80 -120 20 58.7 47.1 QC Sample ID: BWJ1349-MSDI Batch: BWJ1349 QC Source Sample: XXXXXXX-XX Date Prepared: 10/27/2022 Date Analyzed: I 0/28/2022 Units: mg/L Sulfate 108 0.203 80 -120 20 63.1 51.2 QC Sample ID: BWJ1349-MSD2 Batch: BWJ1349 QC Source Sample: XXXXXXX-XX Date Prepared: 10/27/2022 Date Analyzed: 10/28/2022 Units: mg/L Sulfate 32.3 0.251 80 -120 20 1550 1540 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. CtF WO#: 22J1153 www.ChemtechFord.com Spk Value MRL DF 1000 110 1.00 100 11.0 1.00 100 11.0 1.00 100 11.0 1.00 100 11.0 1.00 100 11.0 1.00 100 11.0 1.00 11.1 1.11 1.00 11.1 1.11 1.00 11.1 1.11 1.00 50.0 5.50 1.00 Page 44 of 53 Analyte QC Sample ID: BWJ0971-BLKI Date Prepared: I 0/20/2022 Ammonia as N QC Sample ID: BWJ0971-BS1 Date Prepared: 10/20/2022 Ammonia as N QC Sample ID: BWJ0971-MSI Date Prepared: 10/20/2022 Ammonia as N QC Sample ID: BWJ0971-MSD1 Date Prepared: I 0/20/2022 Ammonia as N CtF WO#: 22J1153 www.ChemtechFord.com QC Report for Work Order (WO) -22J1153 %Rec RPD Limits RPD Max Result Source Cone Blank -EPA 350.1 Batch: BWJ0971 Date Analyzed: 10/27/2 022 Units: mg/L ND LCS -EPA 350.1 Batch: BWJ0971 Date Analyzed: 10/27/2022 Units: mg/L 95.3 90 -110 0.953 Matrix Spike -EPA 350.1 Batch: BWJ0971 QC Source Sample: 2211153-01 Date Analyzed: 10/27/2022 Units: mg/L 114 80 -120 1.60 0.458 Matrix Spike Dup -EPA 350.1 Batch: BWJ0971 QC Source Sample: 2211153-01 Date Analyzed: I 0/27 /2022 Units: mg/L 110 2.78 80 -120 20 1.55 0.458 SpkValue MRL DF 0.0500 1.00 1.00 0.0500 1.00 1.00 0.100 2.00 1.00 0.100 2.00 Page 45 of 53 QC Report for Work Order (WO) -22J1153 Analyte %Rec RPO Limits RPD Max Result Source Cone Blank -EPA 353.2 QC Sample ID: BWJ0849-BLK1 Batch: BWJ0849 Date Prepared: I 0/18/2022 Date Analyzed: 10/18/2022 Units: Nitrate + Nitrite, Total, as N ND LCS -EPA 353.2 QC Sample ID: BWJ0849-BS1 Batch: BWJ0849 Date Prepared: 10/18/2022 Date Analyzed: 10/18/2022 Units: Nitrate + Nitrite, Total, as N 96.5 80-120 1.93 Matrix Spike -EPA 353.2 QC Sample ID: BWJ0849-MS1 Batch: BWJ0849 QC Source Sample: 2211153-01 Date Prepared: 10/18/2022 Date Analyzed: 10/18/2022 Units: Nitrate+ Nitrite, Total, as N 96.7 80 -120 0.967 ND QC Sample ID: BWJ0849-MS2 Batch: BWJ0849 QC Source Sample: 2211153-02 Date Prepared: 10/18/2022 Date Analyzed: 10/18/2022 Units: Nitrate + Nitrite, Total, as N 106 80 -120 3.96 2.90 Matrix Spike Dup -EPA 353.2 QC Sample ID: BWJ0849-MSD1 Batch: BWJ0849 QC Source Sample: 2211153-01 Date Prepared: 10/18/2022 Date Analyzed: 10/18/2022 Units: Nitrate + Nitrite, Total, as N 100 3.75 80 -120 20 1.00 ND QC Sample ID: BWJ0849-MSD2 Batch: BWJ0849 QC Source Sample: 2211153-02 Date Prepared: 10/18/2022 Date Analyzed: 10/18/2022 Units: Nitrate + Nitrite, Total, as N 124 4.39 80 -120 20 4.14 2.90 QM-12 -The MSD recovery was outside acceptance limits, but passed duplicate spike acceptance criteria. The batch was accepted based on the acceptability of the MS. CtF WO#: 22J1153 www.ChemtechFord.com mg/L mg/L mg/L mg/L mg/L mg/L Spk Value MRL DF 0.100 1.00 2.00 0.100 1.00 1.00 · 0.100 1.00 1.00 0.100 1.00 1.00 0.100 1.00 1.00 0.100 1.00 Page 46 of 53 QC Report for Work Order (WO) -22J1153 Analyte %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 8260D /5030A QC Sample ID: BWJ0956-BLK1 Batch: BWJ0956 Date Prepared: 10/19/2022 Date Analyzed: 10/19/2022 Units: ug/L Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 LCS -EPA 8260D /5030A QC Sample ID: BWJ0956-BS1 Batch: BWJ0956 Date Prepared: 10/19/2022 Date Analyzed: 10/19/2022 Units: ug/L Acetone 86.9 70 -130 86.9 100 10.0 1.00 Benzene 97.6 70 -130 9.76 10.0 1.0 1.00 Carbon Tetrachloride 90.3 70 -130 9.03 10.0 1.0 1.00 Chloroform 94.6 70 -130 9.46 10.0 1.0 1.00 Chloromethane 119 70-130 11.9 10.0 1.0 1.00 Methyl Ethyl Ketone 85.3 70-130 85.3 100 10.0 1.00 Methylene Chloride 95.8 70-130 9.58 10.0 1.0 1.00 Naphthalene 89.6 70 -130 8.96 10.0 1.0 1.00 Tetrahydrofuran 106 70 -130 10.6 10.0 1.0 1.00 Toluene 96.2 70 -130 9.62 10.0 1.0 1.00 Xylenes, total 95.9 70 -130 28.8 30.0 1.0 1.00 Matrix Spike -EPA 8260D /5030A QC Sample ID: BWJ0956-MS1 Batch: BWJ0956 QC Source Sample: 2211153-01 Date Prepared: 10/19/2022 Date Analyzed: 10/19/2022 Units: ug/L Acetone 86.4 70 -130 432 ND 500 50.0 1.00 Benzene 93.3 70 -130 46.6 ND 50.0 5.0 1.00 Carbon Tetrachloride 86.5 70 -130 43.2 ND 50.0 5.0 1.00 Chloroform 91.6 70 -130 45.8 ND 50.0 5.0 1.00 Chloromethane 113 70 -130 56.6 ND 50.0 5.0 1.00 Methyl Ethyl Ketone 80.6 70 -130 403 ND 500 50.0 1.00 Methylene Chloride 91 .5 70 -130 45.8 ND 50.0 5.0 1.00 Naphthalene 84.6 70 -130 42.3 ND 50.0 5.0 1.00 Tetrahydrofuran 103 70 · 130 51.4 ND 50.0 5.0 1.00 Toluene 91 .5 70 -130 45.8 ND 50.0 5.0 1.00 Xylenes, total 89.7 70 -130 135 ND 150 5.0 1.00 Matrix Spike Dup -EPA 8260D /5030A QC Sample ID: BWJ0956-MSD1 Batch: BWJ0956 QC Source Sample: 2211153-01 Date Prepared: 10/19/2022 Date Analyzed: 10/19/2022 Units: ug/L Acetone 87.7 1.48 70 -130 20 438 ND 500 50.0 1.00 Benzene 91 .8 1.62 70 -130 20 45.9 ND 50.0 5.0 1.00 Carbon Tetrachloride 82.3 4.98 70 • 130 20 41 .2 ND 50.0 5.0 1.00 Chloroform 91 .1 0.547 70 · 130 20 45.6 ND 50.0 5.0 1.00 Chloromethane 107 5.26 70 -130 20 53.6 ND 50.0 5.0 1.00 Methyl Ethyl Ketone 83.6 3.69 70 -130 20 418 ND 500 50.0 1.00 Methylene Chloride 92.2 0.762 70 -130 20 46.1 ND 50.0 5.0 1.00 CtF WO#: 22J1153 www.ChemtechFord.com Page 47 of 53 Analyte QC Sample ID: BWJ0956-MSDI Date Prepared: 10/19/2022 Naphthalene Tetrahydrofuran Toluene Xylenes, total CtF WO#: 22J1153 www.ChemtechFord.com QC Report for Work Order (WO) -22J1153 %Rec RPD limits RPD Max Result Source Cone Matrix Spike Dup -EPA 8260D /5030A (cont.) Batch: BWJ0956 QC Source Sample: 22Jll53-01 Date Analyzed: 10/19/2022 Units: ug/L 87.6 3.48 70 -130 20 43.8 ND 105 2.31 70 -130 20 52.6 ND 90.0 1.65 70 -130 20 45.0 ND 89.9 0.186 70 -130 20 135 ND SpkValue MRL DF 50.0 5.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 150 5.0 1.00 Page 48 of 53 Analyte QC Sample ID: BWJ0908-BLK1 Date Prepared: 10/19/2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) QC Sample ID: BWJ0908-DUP1 Date Prepared: 10/19/2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Alkalinity -Total (as CaCO3) QC Sample ID: BWJ0908-BS1 Date Prepared: 10/19/2022 Alkalinity -Total (as CaCO3) CtF WO#: 22J1153 www.ChemtechFord.com QC Report for Work Order (WO) -22J1153 %Rec RPO Limits RPO Max Result Source Cone Blank -SM 2320 B Batch: BWJ0908 Date Analyzed: 10/19/2022 Units: mg/L ND ND Duplicate -SM 2320 B Batch: BWJ0908 QC Source Sample: 2211153-01 Date Analyzed: 10/19/2022 Units: mg/L 4.53 20 300 314 20 ND ND 4.53 20 300 314 LCS -SM 2320 B Batch: BWJ0908 Date Analyzed: 10/19/2022 Units: mg/L 95.4 90 -110 225 Spk Value MRL OF 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1,00 1.0 1.00 236 1.0 1.00 Page 49 of 53 Analyte QC Sample ID: BWJ0668-BLK1 Date Prepared: 10/13/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ0805-BLK1 Date Prepared: 10/17/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ0857-BLK1 Date Prepared: l 0/18/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ0668-DUP1 Date Prepared: 10/13/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ0668-DUP2 Date Prepared: l 0/13/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ0805-DUP1 Date Prepared: l O/l 7 /2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ0805-DUP2 Date Prepared: 10/17/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ0857-DUP1 Date Prepared: 10/18/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ0857-DUP2 Date Prepared: l 0/ 18/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ0668-BS1 Date Prepared: 10/13/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ0805-BS1 Date Prepared: 1 O/l 7 /2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ0857-BS1 Date Prepared: 10/18/2022 Total Dissolved Solids (TDS) CtF WO#: 22J1153 www.ChemtechFord.com QC Report for Work Order (WO) -22J1153 %Rec RPO Limits RPD Max Result Source Cone Blank -SM 2540 C Batch: BWJ0668 Date Analyzed: 10/17/2022 Units: mg/L ND Batch: BWJ0805 Date Analyzed: 10/17/2022 Units: mg/L ND Batch: BWJ0857 Date Analyzed: l 0/1 8/2022 Units: mg/L ND Duplicate -SM 2540 C Batch: BWJ0668 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/17/2022 Units: mg/L 0.7 10 552 556 Batch: BWJ0668 QC Source Sample: 2211153-0 l Date Analyzed: l O/l 7 /2022 Units: mg/L 0.2 10 2660 2660 Batch: BWJ0805 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/17/2022 Units: mg/L 0 10 644 644 Batch: BWJ0805 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/17/2022 Units: mg/L 10 368 372 Batch: BWJ0857 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/18/2022 Units: mg/L 0 10 236 236 Batch: BWJ0857 QC Source Sample: XXXXXXX-XX Date Analyzed: l 0/18/2022 Units: mg/L 0.5 10 864 868 LCS -SM 2540 C Batch: BWJ0668 Date Analyzed: 10/l 7 /2022 Units: mg/L 101 90 -110 404 Batch: BWJ0805 Date Analyzed: 1 O/l 7 /2022 Units: mg/L 102 90 -110 408 Batch: BWJ0857 Date Analyzed: 10/18/2022 Units: mg/L 99 90 -110 396 SpkValue MRL DF 20 1.00 20 1.00 10 1.00 20 1.00 20 1.00 20 1.00 20 1.00 20 1.00 20 1.00 400 20 1.00 400 20 1.00 400 20 1.00 Page 50 of 53 Surrogates Report for Work Order (WO) -22J1153 QCID Analyte BWJ0956-BLK1 1,2-Dichloroethane-d4 BWJ0956-BLK1 4-Bromofluorobenzene BWJ0956-BLK1 Toluene-dB BWJ0956-BS1 1,2-Dichloroethane-d4 BWJ0956-BS1 4-Bromofluorobenzene BWJ0956-BS1 Toluene-dB BWJ0956-MS1 1,2-Dichloroethane-d4 BWJ0956-MS1 4-Bromofluorobenzene BWJ0956-MS1 Toluene-dB BWJ0956-MSD1 1,2-Dichloroethane-d4 BWJ0956-MSD1 4-Bromofluorobenzene BWJ0956-MSD1 Toluene-dB CtF WO#: 22J1153 www.ChemtechFord.com %Rec LCL UCL Result Blank -EPA 8260D /5030A 98.5 64.2 126 9.85 97.4 71.4 125 9.74 100 63.2 129 10.0 LCS -EPA 8260D /5030A 97.2 64.2 126 9.72 95.9 71.4 125 9.59 100 63.2 129 10.0 Matrix Spike -EPA 8260D /5030A 96.3 64.2 126 48.2 96.6 71.4 125 48.3 102 63.2 129 50.8 Matrix Spike Dup -EPA 8260D /5030A 98.1 64.2 126 49.0 96.4 71.4 125 48.2 100 63.2 129 50.0 SpkValue Batch OF 10.0 BWJ0956 1.00 10.0 BWJ0956 1.00 10.0 BWJ0956 1.00 10.0 BWJ0956 1.00 10.0 BWJ0956 1.00 10.0 BWJ0956 1.00 50.0 BWJ0956 1.00 50.0 BWJ0956 1.00 50.0 BWJ0956 1.00 50.0 BWJ0956 1.00 50.0 BWJ0956 1.00 50.0 BWJ0956 1.00 Page 51 of 53 Surrogate Recoveries (Field Samples) LabNumber Analyte 8260 Low Level Volatiles 22J1153-01 4-Bromofluorobenzene 22J1153-01 Toluene-dB 22J1153-01 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22J 1153-02 1,2-Dichloroethane-d4 22J1153-02 22J1153-02 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22J 1153-03 1,2-Dichloroethane-d4 22J1153-03 22J1153-03 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22J1153-04 4-Bromofluorobenzene 22J1153-04 22J1153-04 Toluene-dB 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22J1153-05 4-Bromofluorobenzene 22J1153-05 22J1153-05 Toluene-dB 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22J 1153-06 1,2-Dichloroethane-d4 22J1153-06 22J1153-06 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22J 1153-07 1,2-Dichloroethane-d4 22J1153-07 22J1153-07 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22J1153-08 Toluene-dB 22J1153-08 4-Bromofluorobenzene CtF WO#: 22J1153 www.ChemtechFord.com Result 9.68 10.0 9.72 9.73 9.62 10.0 9.56 9.75 9.93 9.53 10.0 9.73 9.68 9.88 10.0 10.0 9.62 10.1 9.91 9.62 10.0 9.96 9.81 Spklvl 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 %Rec 96.8 100 97.2 97.3 96.2 100 95.6 97.5 99.3 95.3 100 97.3 96.8 98.8 100 100 96.2 101 99.1 96.2 100 99.6 98.1 LCL UCL Qualifier 71.4 125 63.2 129 64.2 126 64.2 126 71.4 125 63.2 129 64.2 126 71.4 125 63.2 129 71.4 125 63.2 129 64.2 126 71.4 125 63.2 129 64.2 126 64.2 126 71.4 125 63.2 129 64.2 126 71.4 125 63.2 129 63.2 129 71.4 125 Page 52 of 53 22J1153-08 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22J1153-09 1,2-Dichloroethane-d4 22J1153-09 22J1153-09 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22J 1153-10 1,2-Dichloroethane-d4 22J1153-10 22J1153-10 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22J1153-11 Toluene-dB 22J1153-11 22J1153-11 1,2-Dichloroethane-d4 4-Bromofluorobenzene 8260 Low Level Volatiles 22J 1153-12 Toluene-dB 22J1153-12 22J1153-12 1,2-Dichloroethane-d4 4-Bromofluorobenzene 8260 Low Level Volatiles 22J 1153-13 1,2-Dichloroethane-d4 22J1153-13 22J1153-13 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22J1153-14 1,2-Dichloroethane-d4 22J1153-14 22J1153-14 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22J1153-15 Toluene-dB 22J1153-15 22J1153-15 1,2-Dichloroethane-d4 4-Bromofluorobenzene CtF WO#: 22J1153 www.ChemtechFord.com 9.83 10.1 9.50 10.1 10.1 9.43 10.0 10.0 10.0 9.81 10.0 10.1 9.57 9.83 9.66 10.0 9.96 9.59 10.0 10.0 9.58 9.71 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 98.3 101 95.0 101 101 94.3 100 100 100 98.1 100 101 95.7 98.3 96.6 100 99.6 95.9 100 100 95.8 97.1 64.2 126 64.2 126 71.4 125 63.2 129 64.2 126 71.4 125 63.2 129 63.2 129 64.2 126 71.4 125 63.2 129 64.2 126 71.4 125 64.2 126 71.4 125 63.2 129 64.2 126 71.4 125 63.2 129 63.2 129 64.2 126 71.4 125 Page 53 of 53 9632 South 500 West CHEMTECH-FORD L/,13O~1\T0 RI ES 11/10/2022 Work Order: 22J 1703 Project: 4th Quarter Ground Water 2022 Energy Fuels Resources, Inc. Attn: Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Client Service Contact: 801 .262. 7299 The analyses presented on this report \\/ere performed in accordance with the National Environmental Laboratory-Accreditation Program (NELAP) unless noted in the comments, flags, or case narrative. If the report is to be used for regulatory compliance, it should be presented in its entirety, and not be altered. Approved By: Melissa Connolly, Project Manager Sandy, Utah 84070 801.262 7299 Main 866.792.0093 Fax Serving the lntermountain West since 1953 www.ChemtechFord.com Page 1 of 47 CHEMTECH-FORD LABOAATORIES Energy Fuels Resources, Inc. Project: 4th Quarter Ground Water 2022 Project Manager: Tanner Holliday Laboratory ID 22J1703-01 22J1703-02 22J1703-03 22J1703-04 22J1703-05 22J1703-06 22J1703-07 22J1703-08 22J1703-09 22J1703-10 22J1703-11 Sample Name MW-17_ 10172022 MW-19_ 10172022 MW-18_10182022 MW-40_ 10182022 MW-01_10192022 MW-03A_ 10192022 MW-22_ 10192022 MW-27 _ 10192022 MW-02_ 10202022 MW-39 _ 10202022 Trip Blank Work Order Report Narrative Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions There are no corrective actions associated with this work order. Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 22J1703 Page 2 of 47 CHEMTECH-FORD LABOR,\T0RIES Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Certificate of Analysis Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations ND= Not detected at the corresponding Minimum Reporting Limit (MRL). PO#: Receipt: 10/21/22 10:57@ -0.9 °C Date Reported: 11/10/2022 Project Name: 4th Quarter Ground Water 2022 1 mg/L = one milligram per liter or 1 mg/kg= one milligram per kilogram = 1 part per million. 1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram= I part per billion. 1 ng/L = one nanogram per liter or l ng/kg = one nano gram per kilogram = I part per trillion. Project Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 22J1703 Page 24 of 47 l 1 lb )3 44 ,.. ') 5 ~6 1 7 ~8 19 } 10 American West 11-, il D3 Analytical Laboratories J 463W.3600S. SalllakeCily,UT 84115 Phone# (801) 263-8686 Toll Free# (8881 263-a686 L~ Fax# (801) 263-13687 Email awal@awal-labs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: Email: thoWclay@;eneTgyfaela.com; KWelDel@;energyfoela.com Project Name: 4th Quarter Ground Water 2022 Project#: PO#: Sampler Name: Tanner Holliday Time Samele ID: Date Sam oled Samoled MW-17_10172022 10/17/2022 1100 MW-19_10172022 10/17/2022 1425 MW-18_10182022 10/18/2022 1245 MW-40_10182022 10/18/2022 1120 MW-D1_10192022 10/19/2022 1010 MW-03A_10192022 -10/19/2022 800 MW-22_10192022 10/19/2022 1320 MW-27 _10192022 10/19/2022 1430 MW-02_10202022 10/20/2022 910 MW-39_10202022 10/20/2022 1030 I CHAIN OF CUSTODY All analysis will be conducted using NELAP accredited melhods and all dela will be reported using AWAL's standard analyte llsls and reporting limlts (POL) unless specifically requested otherwise on this Chain of Custody and/or attached documentation. QC Level: I Tum Around Time: Unless other arrangements have been made, signed reports will be emailed by 5:00 pm on 3 Standard the day they are due X Include EDD: o· LOCUS UPLOAD ::;: "' u EXCEL oli tlD X Field Filtered For: ~ ::i: ::;: DINolved Metal& ...... C: ui ::;: :,l 't-C'l .0 of ~ 0.. z For Compliance With: 0 .; d" □ NELAP 0 [%.. N □ RCRA a' C'l :i > □ CWA 0 ;:::- 0 0 u ::i □ SOWA ~ C') 0 ...... ii:i' 0 □ ELAP/A2LA 0 ... ~ u r:5 0 □ NLLAP 1/) 0 (I) ;:;--0 C'l -; .: □ Non-Compliance C') ~ C') u i:::· ~ ... ~ ... □ Other: 0 ::!:. 0 -c:i oli D' ~ !2. Q D' 'S :a u < .. 0 " X 0 ..,. 0 Cl IO C: :s (') a 0 't-Cl "Cl ., .; -! C'l ]i .. 0 1/) fll 1/) iii ! Cil (I) ~ ::;; Known Hazards C: li!: ::!:. tf ~ ,,; 0 ., --0 z IQ • C) ci N ! m 'S • < u & 'o E 0 t ~ • a g .. l!; u iS 0 Samele Comments .. Cf) .. 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X AWAL Lab Sample Set# Page 1 of 1 I""" Da,o Laboratory Use Only Samples Were: 1 &na delivered 2 Ambient or Chilled 3 Temperalure -li-c 4 Received Broken/Leaking (lmproperty Sealed) y N 5 Property Presenred y N Checked al bench y N 6 Received Wll!lln Holding Times y N COC Tape Was: '(J)' on Outer Package N NA 2 Unbroken on Outer Package y N NA 3 Present on Sample y N NA 4 Unbroken on sample y N NA Discrepancies Between Sample Labels and coc Record? y N I TRIPBLAl'fK \ 12 10/17/2022 1100 3 w n X -•~ Relinquished by: --\ '/ ,1 / ...,,/ 10/;;JJ/~ RcceivO<lby: . ,//.L--" Dalw n 1/ 1., L Special Instructions: Stonalure ---lc;o,nature /,.,.,,-? • --1:"'""'r J oll:A11.1.J' . 'rrt ".ft<; ITlm• II'\ C.( Print Name: IIOD Prtnl Name! Sample containers for metals were field filtered. See the Relinquished by: n Received by: Date Analytical Scope of Work for Reporting Limits and voe analyte ~lnnallJre Skmature [Time: list. or1ntName: PrtntName_: Relinquished by: Received by: Daie: Sianalure Sianalure !Time: UP~ Print Name: l'rintName: Relinquished by: Received by: oa,o: -· .. -1Z3W951A03651993~4 Sianalure Sianalure Time: 1Z187Y4Y03~65538~ Page 25 of 47 Prlnl Name: pn.ntName: I /'/ "7 . ~ Work Order# L,~) \10 ":7 DeJµtery Method: _.P'UPS D USPS CHEMTECH FORD LABORATORIES Sample Receipt FedEx D Ch hC ourier , , • D (._.f Jurier • a Receiving Temperature -' I ° C ~ f ':. .& l! !5 t: i i ! ~ E .!! i li r; ..... ~ r Ch ch Lo i -i Ci 6, :!:! -· -1 .J • " ..., ~ .... J LI :.A. ., , • -, • ~ -":. --T •• emte t I "" ~ .s !, Misc _ ~ , 1. -~ 'L, ~. • • .f'. .~ 1 k "& "' l C ,,. .... ·' .. • : -.. ' • ·~ _ .... or i ! , j Volume ~ 1? • 1i · ~ •'. . ·· '. ~ sample # Container Preservative ! J 11 ~ (oz/mll Comments 1JI-I\ vJl:, l 17 t) <» "I ..... IO N I '2:~i"i _ ~? I I 1°')6 1\?y \ 0 1;\~ i I 9/v . .- iv\ i1A 9) ~,i:::, 11 ·p, I Tr:-ef?\') lil-ffL \\.,,1 ~w PiL -. Ah l\ \"' Lfff I CHEMTECH-FORD L,\BORATORl[S Sample Cond.ition (check if yes I n be malched to bottles Plastic Containers A· Plastic Unpreserved B-Miscellaneous Plastic C· Cyanide Qt (Na0HI E· Colilorm/Ecoli/HPC F-Sulride Qt (Zn Acetate) L· Mercury 1631 M· Metals Pint (HN03) N-Nutrient Pint (H2S04) R· Radiological (HN03) S· Sludge Cups/Tubs Q-Plastic Sag Glass Containers D· 62S (Na2S203) G· Glass Unpreserved H· HAAS (NH4CI) J· 508/S15/S25 (Na2S03) K-515.3 Herbicides 0· Oil & Grease (HCI) p. Phenols (H2S04) f. TOC/T0X (H3P04) U-531 (MCAA, Na25203) V-524/THMs (Ascorbic Acid) W· 8260 voe (1:1 HCIJ X-Vial Unpreserved Y· 624/S04 (Na2S203) z. Miscellaneous Glass Page 26 of 47 QC Report for Work Order (WO) -22J1703 Analyte %Rec RPO Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 200.7 QC Sample ID: BWJI 119-BLKl Batch: BWJ1119 Date Prepared: 10/24/2022 Date Analyzed: 10/24/2022 Units: mg/L Calcium, Dissolved ND 0,2 1.00 Iron, Dissolved ND 0.03 1.00 Magnesium, Dissolved ND 0.2 1.00 Potassium, Dissolved ND 0.5 1.00 Sodium, Dissolved ND 0.5 1.00 Tin, Dissolved ND 0.10 1.00 QC Sample ID: BWK0365-BLK1 Batch: BWK0365 Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Calcium, Dissolved ND 0.2 1.00 Magnesium, Dissolved ND 0.2 1.00 Potassium, Dissolved ND 0.5 1.00 Sodium, Dissolved ND 0.5 1.00 LCS -EPA 200.7 QC Sample ID: BWJI 119-BS 1 Batch: BWJ1119 Date Prepared: 10/24/2022 Date Analyzed: 10/24/2022 Units: mg/L Calcium, Dissolved 101 85 -115 10.3 10.2 0.2 1.00 Iron, Dissolved 97.5 85 -115 0.195 0.200 0.02 1.00 Magnesium, Dissolved 101 85 -115 10.3 10.2 0.2 1.00 Potassium, Dissolved 105 85 -115 10.5 10.0 0.5 1.00 Sodium, Dissolved 98.3 85 -115 9.8 10.0 0.5 1.00 Tin , Dissolved 95.7 85 -155 0.19 0.201 0.02 1.00 QC Sample ID: BWK0365-BS1 Batch: BWK0365 Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Calcium, Dissolved 97.9 85 -115 10.0 10.2 0.2 1.00 Magnesium, Dissolved 99.2 85 -115 10.1 10.2 0.2 1.00 Potassium, Dissolved 98.4 85 -115 9,8 10.0 0.5 1.00 Sodium, Dissolved 96.8 85 -115 9.7 10.0 0.5 1.00 Matrix Spike -EPA 200.7 QC Sample ID: BWJl 119-MSl Batch: BWJI 119 QC Source Sample: XXXXXXX-XX Date Prepared: 10/24/2022 Date Analyzed: 10/24/2022 Units: mg/L Calcium, Dissolved 90.6 70 -130 80.3 71.0 10.2 0.2 1.00 Iron, Dissolved 100 70 -130 0.200 ND 0.200 0.02 1.00 Magnesium, Dissolved 98.3 70 -130 36.2 26.2 10.2 0.2 1.00 Potassium, Dissolved 107 70 -130 11.4 0.7 10.0 0.5 1.00 Sodium, Dissolved 96.7 70 -130 22.3 12.7 10.0 0.5 1.00 lin, Dissolved 96.2 70 -130 0.19 ND 0.201 0.02 1.00 QC Sample ID: BWJ1119-MS2 Batch: BWJI 119 QC Source Sample: 22Jl 703-06 Date Prepared: 10/24/2022 Date Analyzed: 10/24/2022 Units: mg/L Calcium, Dissolved 44.6 70 -130 431 426 10.2 0.2 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Iron, Dissolved 88.1 70 -130 0.176 ND 0.200 0.02 1.00 Magnesium, Dissolved 79.6 70 -130 272 264 10.2 0.2 1.00 Potassium, Dissolved 104 70 -130 35.9 25.5 10.0 0.5 1.00 Sodium, Dissolved -786 70 -130 694 773 10.0 0.5 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. CtF WO#: 22J1703 www.ChemtechFord.com Page 27 of 47 QC Report for Work Order (WO) -22J1703 Analyte % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Matrix Spike -EPA 200.7 (cont.) QC Sample ID: BWJI l 19-MS2 Batch: BWJI 119 QC Source Sample: 22Jl 703-06 Date Prepared: I 0/24/2022 Date Analyzed: 10/24/2022 Units: mg/L Tin, Dissolved 97.7 70 -130 0.20 ND 0.201 0.02 1.00 QC Sample ID: BWK0365-MSI Batch: BWK0365 QC Source Sample: XXXXXXX-XX Date Prepared: 11/08/2022 Date Analyzed: I 1/08/2022 Units: mg/L Calcium, Dissolved 99.4 70 -130 53.8 43.7 10.2 0.2 1.00 Magnesium, Dissolved 101 70 -130 29.0 18.8 10.2 0.2 1.00 Potassium, Dissolved 98.8 70 -130 11.9 2.0 10.0 0.5 1.00 Sodium, Dissolved 95.3 70 -130 45.0 35.5 10.0 0.5 1.00 QC Sample ID: BWK0365-MS2 Batch: BWK0365 QC Source Sample: XXXXXXX-XX Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Calcium, Dissolved 162 70 -130 512 496 10.2 0.2 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Magnesium, Dissolved 125 70 -130 171 158 10.2 0.2 1.00 Potassium, Dissolved 106 70 -130 21.4 10.8 10.0 0.5 1.00 Sodium, Dissolved 105 70 -130 372 361 10.0 0.5 1.00 Matrix Spike Dup -EPA 200.7 QC Sample ID: BWJI II9-MSDl Batch: BWJl119 QC Source Sample: XXXXXXX-XX Date Prepared: 10/24/2022 Date Analyzed: 10/24/2022 Units: mg/L Calcium, Dissolved 92.1 0.184 70 -130 20 80.4 71.0 10.2 0.2 1.00 Iron, Dissolved 99.8 0.400 70 -130 20 0.200 ND 0.200 0.02 1.00 Magnesium, Dissolved 99.3 0.257 70 -130 20 36.3 26.2 10.2 0.2 1.00 Potassium, Dissolved 109 1.44 70 -130 20 11.6 0.7 10.0 0.5 1.00 Sodium, Dissolved 97.9 0.553 70 -130 20 22.5 12.7 10.0 0.5 1.00 Tin, Dissolved 101 4.65 70 -130 20 0.20 ND 0.201 0.02 1.00 QC Sample ID: BWJl119-MSD2 Batch: BWJI 119 QC Source Sample: 22Jl 703-06 Date Prepared: 10/24/2022 Date Analyzed: 10/24/2022 Units: mg/L Calcium, Dissolved 273 5.25 70 -130 20 454 426 10.2 0.2 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Iron, Dissolved 97.8 10.4 70 -130 20 0.196 ND 0.200 0.02 1.00 Magnesium, Dissolved 224 5.26 70 -130 20 287 264 10.2 0.2 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Potassium, Dissolved 120 4.18 70 -130 20 37.5 25.5 10.0 0.5 1.00 Sodium, Dissolved -461 4.58 70 -130 20 727 773 10.0 0.5 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Tin, Dissolved 106 8.30 70 -130 20 0.21 ND 0.201 0.02 1.00 QC Sample ID: BWK0365-MSD1 Batch: BWK0365 QC Source Sample: XXXXXXX-XX Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Calcium, Dissolved 106 1.24 70 -130 20 54.5 43.7 10.2 0.2 1.00 Magnesium, Dissolved 106 1.66 70-130 20 29.5 18.8 10.2 0.2 1.00 Potassium, Dissolved 103 3.10 70 -130 20 12.3 2.0 10.0 0.5 1.00 Sodium, Dissolved 102 1.40 70 -130 20 45.7 35.5 10.0 0.5 1.00 QC Sample ID: BWK0365-MSD2 Batch: BWK0365 QC Source Sample: XXXXXXX-XX Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L CtF WO#: 22J1703 www.ChemtechFord.com Page 28 of 47 QC Report for Work Order (WO) -22J1703 Analyte %Rec RPO Limits RPO Max Result Source Cone QC Sample ID: BWK0365-MSD2 Date Prepared: 11/08/2022 Calcium, Dissolved Magnesium, Dissolved Potassium, Dissolved Matrix Spike Dup -EPA 200.7 (cont.) Batch: BWK0365 QC Source Sample: XXXXXXX-XX Date Analyzed: 11/08/2022 Units: 83.9 1.57 70 -130 20 504 496 98.6 1.57 70 -130 20 168 158 106 0.195 70 -130 20 21.3 10.8 Sodium, Dissolved 66.7 1.05 70 -130 20 368 361 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. CtF WO#: 22J1703 www.ChemtechFord.com mg/L Spk Value 10.2 10.2 10.0 10.0 MRL 0.2 0.2 0.5 0.5 OF 1.00 1.00 1.00 1.00 Page 29 of 47 QC Report for Work Order (WO) -22J1703 Analyte % Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 200.8 QC Sample ID: BWJ1231-BLK1 Batch: BWJ1231 Date Prepared: I 0/26/2022 Date Analyzed: I 0/26/2022 Units: mg/L Arsenic, Dissolved ND 0.0050 1.00 Beryllium, Dissolved ND 0.0005 1.00 Cadmium, Dissolved ND 0.0005 1.00 Chromium, Dissolved ND 0.0250 1.00 Cobalt, Dissolved ND 0.010 1.00 Copper, Dissolved ND 0.0100 1.00 Lead, Dissolved ND 0.0010 1.00 Manganese, Dissolved ND 0.0100 1.00 Molybdenum, Dissolved ND 0.0100 1.00 Nickel, Dissolved ND 0.0200 1.00 Selenium, Dissolved ND 0.0050 1.00 Silver, Dissolved ND 0.010 1.00 Thallium, Dissolved ND 0.0005 1.00 Uranium, Dissolved ND 0.0003 1.00 Vanadium, Dissolved ND 0.0150 1.00 Zinc, Dissolved ND 0.0100 1.00 QC Sample ID: BWJ1232-BLK1 Batch: BWJI232 Date Prepared: I 0/26/2022 Date Analyzed: I 0/26/2022 Units: mg/L Arsenic, Dissolved ND 0.0050 1.00 Beryllium, Dissolved ND 0.0005 1.00 Cadmium, Dissolved ND 0.0005 1.00 Chromium, Dissolved ND 0.0250 1.00 Cobalt, Dissolved ND 0.010 1.00 Copper, Dissolved ND 0.0100 1.00 Lead, Dissolved ND 0.0010 1.00 Manganese, Dissolved ND 0.0100 1.00 Molybdenum, Dissolved ND 0.0100 1.00 Nickel, Dissolved ND 0.0200 1.00 Selenium, Dissolved ND 0.0050 1.00 Silver, Dissolved ND 0.010 1.00 Thallium, Dissolved ND 0.0005 1.00 Uranium, Dissolved ND 0.0003 1.00 Vanadium, Dissolved ND 0.0150 1.00 Zinc, Dissolved ND 0.0100 1.00 LCS -EPA 200.8 QC Sample ID: BWJ1231-BS1 Batch: BWJ123 l Date Prepared: 10/26/2022 Date Analyzed: I 0/26/2022 Units: mg/L Arsenic, Dissolved 103 85-115 0.041 0.0400 0.0005 1.00 Beryllium, Dissolved 104 85 -115 0.041 0.0400 0.0005 1.00 Cadmium, Dissolved 102 85-115 0.041 0.0400 0.0002 1.00 Chromium, Dissolved 107 85-115 0.043 0.0400 0.0005 1.00 Cobalt, Dissolved 104 85 -115 0.042 0.0400 0.0005 1.00 Copper, Dissolved 101 85 -115 0.040 0.0400 0.0010 1.00 Lead, Dissolved 101 85 -115 0.040 0.0400 0.0005 1.00 Manganese, Dissolved 104 85 -115 0.042 0.0400 0.0005 1.00 Molybdenum, Dissolved 103 85 -115 0.041 0.0400 0.0005 1.00 Nickel, Dissolved 101 85 -115 0.0403 0.0400 0.0005 1.00 Selenium, Dissolved 102 85 -115 0.041 0.0400 0.0005 1.00 Silver, Dissolved 102 85 -115 0.041 0.0400 0.0005 1.00 Thallium, Dissolved 108 85 -115 0.043 0.0400 0.0002 1.00 CtF WO#: 22J1703 www.ChemtechFord.com Page 30 of 47 QC Report for Work Order (WO) -22J1703 Analyte %Rec RPD Limits RPD Max Result Source Cone SpkValue MRL DF LCS -EPA 200.8 (cont.) QC Sample ID: BWJ1231-BSI Batch: BWJ1231 Date Prepared: I 0/26/2022 Date Analyzed: I 0/26/2022 Units: mg/L Uranium, Dissolved 102 85 -115 0.041 0.0400 0.0003 1.00 Vanadium, Dissolved 107 85 -115 0.043 0.0400 0.0005 1.00 Zinc, Dissolved 100 85 -115 0.040 0.0400 0.0100 1.00 QC Sample ID: BWJ1232-BSI Batch: BWJ1232 Date Prepared: 10/26/2022 Date Analyzed: I 0/26/2022 Units: mg/L Arsenic, Dissolved 99.2 85-115 0.040 0.0400 0.0005 1.00 Beryllium, Dissolved 101 85 -115 0.040 0.0400 0.0005 1.00 Cadmium, Dissolved 99.1 85 -115 0.040 0.0400 0.0002 1.00 Chromium, Dissolved 97.7 85-115 0.039 0.0400 0.0005 1.00 Cobalt, Dissolved 98.5 85-115 0.039 0.0400 0.0005 1.00 Copper, Dissolved 95.2 85 -115 0.038 0.0400 0.0010 1.00 Lead, Dissolved 98.5 85 -115 0.039 0.0400 0.0005 1.00 Manganese, Dissolved 98.9 85 -115 0.040 0.0400 0.0005 1.00 Molybdenum, Dissolved 99.8 85 -115 0.040 0.0400 0.0005 1.00 Nickel, Dissolved 94.0 85 -115 0.0376 0.0400 0.0005 1.00 Selenium, Dissolved 98.8 85 -115 0.040 0.0400 0.0005 1.00 Silver, Dissolved 97.9 85-115 0.039 0.0400 0.0005 1.00 Thallium, Dissolved 104 85 -115 0.042 0.0400 0.0002 1.00 Uranium, Dissolved 95.2 85 -115 0.038 0.0400 0.0003 1.00 Vanadium, Dissolved 102 85 -115 0.041 0.0400 0.0005 1.00 Zinc, Dissolved 94.8 85 -115 0.038 0.0400 0.0100 1.00 Matrix Spike -EPA 200.8 QC Sample ID: BWJ1231-MSI Batch: BWJ123 l QC Source Sample: XXXXXXX-XX Date Prepared: 10/26/2022 Date Analyzed: I 0/26/2022 Units: mg/L Arsenic, Dissolved 111 70 -130 0.060 0.016 0.0400 0.0005 1.00 Beryllium, Dissolved 104 70 -130 0.042 ND 0.0400 0.0005 1.00 Cadmium, Dissolved 101 70 -130 0.041 0.0002 0.0400 0.0002 1.00 Chromium, Dissolved 103 70 -130 0.042 0.001 0.0400 0.0005 1.00 Cobalt, Dissolved 100 70 -130 0.041 0.0005 0.0400 0.0005 1.00 Copper, Dissolved 95.9 70 -130 0.039 0.0006 0.0400 0.0010 1.00 Lead, Dissolved 99.2 70 -130 0.040 ND 0.0400 0.0005 1.00 Manganese, Dissolved 98.7 70 -130 0.064 0.024 0.0400 0.0005 1.00 Molybdenum, Dissolved 104 70 -130 0.046 0.005 0.0400 0.0005 1.00 Nickel, Dissolved 95.2 75 -125 0.0416 0.0035 0.0400 0.0005 1.00 Selenium, Dissolved 118 70 -130 0.050 0.003 0.0400 0.0005 1.00 Silver, Dissolved 100 70 -130 0.040 ND 0.0400 0.0005 1.00 Thallium, Dissolved 106 70 -130 0.045 0.003 0.0400 0.0002 1.00 Uranium, Dissolved 104 70 -130 0.046 0.005 0.0400 0.0003 1.00 Vanadium, Dissolved 107 70 -130 0.043 0.0006 0.0400 0.0005 1.00 Zinc, Dissolved 98.4 70-130 0.159 0.120 0.0400 0.0100 1.00 QC Sample ID: BWJ1231-MS2 Batch: BWJ1231 QC Source Sample: XXXXXXX-XX Date Prepared: I 0/26/2022 Date Analyzed: I 0/26/2022 Units: mg/L Arsenic, Dissolved 107 70 -130 0.060 0.017 0.0400 0.0005 1.00 Beryllium, Dissolved 104 70 -130 0.042 ND 0.0400 0.0005 1.00 Cadmium, Dissolved 100 70 -130 0.040 0.0002 0.0400 0.0002 1.00 Chromium, Dissolved 101 70 -130 0.041 0.001 0.0400 0.0005 1.00 Cobalt, Dissolved 96.9 70 -130 0.039 0.0006 0.0400 0.0005 1.00 Copper, Dissolved 94.0 70 -130 0.038 0.0008 0.0400 0.0010 1.00 Lead, Dissolved 98.5 70 -130 0.039 ND 0.0400 0.0005 1.00 CtF WO#: 22J1703 www.ChemtechFord.com Page 31 of 47 Analyte QC Sample ID: BWJ1231-MS2 Date Prepared: 10/26/2022 Manganese, Dissolved Molybdenum, Dissolved Nickel, Dissolved Selenium, Dissolved Silver, Dissolved Thallium, Dissolved Uranium, Dissolved Vanadium, Dissolved Zinc, Dissolved QC Sample ID: BWJ1232-MS1 Date Prepared: 10/26/2022 Arsenic, Dissolved Beryllium, Dissolved Cadmium, Dissolved Chromium, Dissolved Cobalt, Dissolved Copper, Dissolved Lead, Dissolved Manganese, Dissolved Molybdenum, Dissolved Nickel, Dissolved Selenium, Dissolved Silver, Dissolved Thallium, Dissolved Uranium, Dissolved Vanadium, Dissolved Zinc, Dissolved CtF WO#: 22J1703 www.ChemtechFord.com QC Report for Work Order (WO) -22J1703 %Rec RPD Limits RPDMax Result Source Cone SpkValue MRL DF Matrix Spike -EPA 200.8 (cont.) Batch: BWJ123 l QC Source Sample: XXXXXXX-X:X Date Analyzed: 10/26/2022 Units: mg/L 96.1 70 -130 0.066 0.027 0.0400 0.0005 1.00 104 70 -130 0.047 0.005 0.0400 0.0005 1.00 93.7 75 -125 0.0414 0.0039 0.0400 0.0005 1.00 116 70 -130 0.049 0.003 0.0400 0.0005 1.00 97.1 70 -130 0.039 ND 0.0400 0.0005 1.00 105 70 -130 0.045 0.003 0.0400 0.0002 1.00 102 70 -130 0.046 0.006 0.0400 0.0003 1.00 103 70 -130 0.042 0.0006 0.0400 0.0005 1.00 97.2 70 -130 0.178 0.139 0.0400 0.0100 1.00 Batch: BWJ1232 QC Source Sample: 22Jl 703-06 Date Analyzed: 10/26/2022 Units: mg/L 110 70 -130 0.044 ND 0.0400 0.0005 1.00 95.5 70 -130 0.039 0.0003 0.0400 0.0005 1.00 94.3 70 -130 0.038 0.0007 0.0400 0.0002 1.00 92.9 70 -130 0.039 0.002 0.0400 0.0005 1.00 90.2 70 -130 0.037 0.0008 0.0400 0.0005 1.00 81.5 70 -130 0.035 0.003 0.0400 0.0010 1.00 89.7 70 -130 0.036 ND 0.0400 0.0005 1.00 87.0 70 -130 0.083 0.049 0.0400 0.0005 1.00 108 70 -130 0.044 0.0004 0.0400 0.0005 1.00 82.1 75 -125 0.0392 0.0063 0.0400 0.0005 1.00 120 70 -130 0.145 0.097 0.0400 0.0005 1.00 87.5 70 -130 0.035 ND 0.0400 0.0005 1.00 97.4 70 -130 0.039 0.0004 0.0400 0.0002 1.00 93.9 70 -130 0.056 0.018 0.0400 0.0003 1.00 101 70 -130 0.041 0.0007 0.0400 0.0005 1.00 80.8 70 -130 0.046 0.014 0.0400 0.0100 1.00 Page 32 of 47 Analyte QC Sample ID: BWJI 186-BLKl Date Prepared: 10/25/2022 Mercury, Dissolved QC Sample ID: BWJ1186-BSI Date Prepared: 10/25/2022 Mercury, Dissolved QC Sample ID: BWJ1186-MS1 Date Prepared: 10/25/2022 Mercury, Dissolved QC Sample ID: BWJ1186-MS2 Date Prepared: 10/25/2022 Mercury, Dissolved QC Sample ID: BW11186-MSD1 Date Prepared: 10/25/2022 Mercury, Dissolved QC Sample ID: BWJI 186-MSD2 Date Prepared: 10/25/2022 Mercury, Dissolved CtF WO#: 22J1703 www.ChemtechFord.com QC Report for Work Order (WO) -22J1703 % Rec RPO Limits RPO Max Result Source Cone Blank -EPA 245.1 Batch: BWJI 186 Date Analyzed: 10/26/2022 Units: mg/L ND LCS -EPA 245.1 Batch: BWJI 186 Date Analyzed: I 0/26/2022 Units: mg/L 98.9 85 -115 0.00494 Matrix Spike -EPA 245.1 Batch: BW11186 QC Source Sample: 2211703-01 Date Analyzed: 10/26/2022 Units: mg/L 104 75 -125 0.00521 ND Batch: BWJl 186 QC Source Sample: 2211703-06 Date Analyzed: I 0/26/2022 Units: mg/L 103 75 -125 0.00513 ND Matrix Spike Dup -EPA 245.1 Batch: BW11186 QC Source Sample: 2211703-01 Date Analyzed: 10/26/2022 Units: mg/L 107 2.47 75 -125 20 0.00534 ND Batch: BW11186 QC Source Sample: 2211703-06 Date Analyzed: 10/26/2022 Units: mg/L 110 7.08 75 -125 20 0.00550 ND Spk Value MRL OF 0.00050 1.00 0.00500 0.00015 1.00 0.00500 0.00015 1.00 0.00500 0.00015 1.00 0.00500 0.00015 1.00 0.00500 0.00015 1.00 Page 33 of 47 QC Report for Work Order (WO) -22J1703 Analyte % Rec RPD Limits RPDMax Result Source Cone Spk Value MRL DF Blank -EPA 300.0 QC Sample ID: BWJl199-BLK1 Batch: BWJI 199 Date Prepared: 10/25/2022 Date Analyzed: 10/25/2022 Units: mg/L Chloride ND 1.00 1.00 Sulfate ND 1.00 1.00 QC Sample ID: BWJl205-BLK1 Batch: BWJ1205 Date Prepared: 10/25/2022 Date Analyzed: 10/25/2022 Units: mg/L Chloride ND 1.00 1.00 Sulfate ND 1.00 1.00 QC Sample ID: BWJl257-BLK1 Batch: BWJl257 Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: mg/L Chloride ND 1.00 1.00 Fluoride ND 0.100 1.00 Sulfate ND 1.00 1.00 QC Sample ID: BWJl470-BLK1 Batch: BWJ1470 Date Prepared: 10/31/2022 DateAnalyzed: 11/01/2022 Units: mg/L Chloride ND 1.00 1.00 QC Sample ID: BWK0078-BLK1 Batch: BWK0078 Date Prepared: 11/02/2022 Date Analyzed: 11/02/2022 Units: mg/L Fluoride ND 0.100 1.00 QC Sample ID: BWK0427-BLK1 Batch: BWK0427 Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Chloride ND 1.00 1.00 Sulfate ND 1.00 1.00 LCS -EPA 300.0 QC Sample ID: BWJl199-BS1 Batch: BWJI 199 Date Prepared: 10/25/2022 Date Analyzed: 10/25/2022 Units: mg/L Chloride 101 90 -110 50.6 50.0 1.00 1.00 Sulfate 100 90 -110 50.0 50.0 1.00 1.00 QC Sample ID: BWJl205-BS1 Batch: BWJ1205 Date Prepared: 10/25/2022 Date Analyzed: 10/25/2022 Units: mg/L Chloride 102 90 -110 50.8 50.0 1.00 1.00 Sulfate 100 90 -110 50.2 50.0 1.00 1.00 QC Sample ID: BWJl257-BS1 Batch: BWJl257 Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: mg/L Chloride 99.4 90 -110 49.7 50.0 1.00 1.00 Fluoride 97.2 90 -110 4.86 5.00 0.100 1.00 Sulfate 98.4 90 -110 49.2 50.0 1.00 1.00 QC Sample ID: BWJl470-BS1 Batch: BWJl470 Date Prepared: 10/31/2022 Date Analyzed: 11/01/2022 Units: mg/L Chloride 101 90 -110 50.5 50.0 1.00 1.00 QC Sample ID: BWK0078-BS1 Batch: BWK0078 Date Prepared: 11/02/2022 Date Analyzed: 11/02/2022 Units: mg/L Fluoride 95.8 90 -110 4.79 5.00 0.100 1.00 QC Sample ID: BWK0427-BS1 Batch: BWK0427 Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Chloride 101 90 -110 50.5 50.0 1.00 1.00 Sulfate 101 90 -110 50.3 50.0 1.00 1.00 CtF WO#: 22J1703 www.ChemtechFord.com Page 34 of 47 QC Report for Work Order (WO) -22J1703 Analyte % Rec RPD Limits RPD Max Result Source Cone Matrix Spike -EPA 300.0 QC Sample ID: BWJI 199-MS 1 Batch: BWJI 199 QC Source Sample: 2211703-06 Date Prepared: 10/25/2022 Date Analyzed: 10/25/2022 Units: mg/L Chloride 94.5 80 -120 244 55.5 Sulfate 70.9 80 -120 2660 2520 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWJI l 99-MS2 Batch: BWJl 199 QC Source Sample: XXXXXXX-XX Date Prepared: 10/25/2022 Date Analyzed: 10/25/2022 Units: mg/L Chloride 62.6 80 -120 261 254 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Sulfate 110 80 -120 407 395 QC Sample ID: BWJ1205-MS1 Batch: BWJ1205 QC Source Sample: XXXXXXX-XX Date Prepared: 10/25/2022 Date Analyzed: 10/26/2022 Units: mg/L Chloride 199 80 -120 2040 1840 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Sulfate 4.37 80 -120 1260 1260 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWJ1205-MS2 Batch: BWJ1205 QC Source Sample: XXXXXXX-XX Date Prepared: 10/25/2022 Date Analyzed: 10/26/2022 Units: mg/L Chloride 612 80 -120 11700 10500 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Sulfate 113 80 -120 596 370 QC Sample ID: BWJ1257-MS1 Batch: BWJ1257 QC Source Sample: 2211703-06 Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: mg/L Chloride 99.9 80 -120 539 39.9 Fluoride 94.8 80 -120 47.4 ND Sulfate 161 80 -120 3100 2300 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWJ1257-MS2 Batch: BWJ1257 QC Source Sample: XXXXXXX-XX Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: mg/L Chloride 116 80 -120 11600 ND Fluoride 94.2 80 -120 942 ND Sulfate 98.7 80 -120 10900 1000 QC Sample ID: BWJ1470-MS1 Batch: BWJ1470 QC Source Sample: XXXXXXX-XX Date Prepared: 10/31/2022 Date Analyzed: 11/01/2022 Units: mg/L Chloride 56.3 80 -120 2860 2290 QM-RPD -The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BWJ1470-MS2 Date Prepared: 10/31/2022 Chloride CtF WO#: 22J1703 www.ChemtechFord.com Batch: BWJ1470 QC Source Sample: XXXXXXX-XX Date Analyzed: 11/01/2022 Units: mg/L 97.1 80-120 10.8 ND SpkValue MRL DF 200 22.0 1.00 200 22.0 1.00 11.1 1.11 1.00 11.1 1.11 1.00 100 11.0 1.00 100 11.0 1.00 200 22.0 1.00 200 22.0 1.00 500 55.0 1.00 50.0 5.50 1.00 500 55.0 1.00 10000 1100 1.00 1000 110 1.00 10000 1100 1.00 1000 110 1.00 11.1 1.11 1.00 Page 35 of 47 QC Report for Work Order (WO) -22J1703 Analyte % Rec RPD Limits RPD Max Result Source Cone Matrix Spike -EPA 300.0 (cont.) QC Sample ID: BWK0078-MS1 Batch: BWK0078 QC Source Sample: 2211703-06 Date Prepared: 11/02/2022 Date Analyzed: 11/02/2022 Units: mg/L Fluoride 88.7 80 -120 5.80 1.36 QC Sample ID: BWK0078-MS2 Batch: BWK0078 QC Source Sample: XXXXXXX-XX Date Prepared: 11/02/2022 Date Analyzed: 11/02/2022 Units: mg/L Fluoride 71.3 80 -120 0.890 0.098 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO QC Sample ID: BWK0427-MSI Batch: BWK0427 QC Source Sample: 2211703-06 Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Chloride 97.4 80 -120 543 56.4 Sulfate 98.9 80 -120 4010 3520 Matrix Spike Dup -EPA 300.0 QC Sample ID: BW11199-MSDI Batch: BW11199 QC Source Sample: 2211703-06 Date Prepared: 10/25/2022 Date Analyzed: 10/25/2022 Units: mg/L Chloride 93.4 0.882 80 -120 20 242 55.5 Sulfate 88.3 1.30 80 -120 20 2700 2520 QC Sample ID: BWJI 199-MSD2 Batch: B WJI 199 QC Source Sample: XXXXXXX-XX Date Prepared: 10/25/2022 Date Analyzed: 10/25/2022 Units: mg/L Chloride 63.1 0.0219 80 -120 20 261 254 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Sulfate 101 0.255 80 -120 20 406 395 QC Sample ID: BWJ1205-MSDI Batch: BW11205 QC Source Sample: XXXXXXX-XX Date Prepared: 10/25/2022 Date Analyzed: 10/26/2022 Units: mg/L Chloride 180 0.907 80 -120 20 2020 1840 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Sulfate -7.19 0.919 80 -120 20 1250 1260 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWJ1205-MSD2 Batch: BW11205 QC Source Sample: XXXXXXX-XX Date Prepared: I 0/25/2022 Date Analyzed: 10/26/2022 Units: mg/L Chloride -148 13.9 80 -120 20 10200 10500 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Sulfate 88.4 8.54 80 -120 20 547 370 QC Sample ID: BWJ1257-MSD1 Batch: BWJ1257 QC Source Sample: 2211703-06 Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: mg/L Chloride 98.3 1.43 80 -120 20 532 39.9 Fluoride 93.5 1.38 80 -120 20 46.8 ND Sulfate 160 0.290 80 -120 20 3100 2300 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWJ1257-MSD2 Date Prepared: l 0/26/2022 CtF WO#: 22J1703 www.ChemtechFord.com Batch: BW11257 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/26/2022 Units: mg/L Spk Value MRL DF 5.00 0.550 1.00 1.11 0.111 1.00 500 55.0 1.00 500 55.0 1.00 200 22.0 1.00 200 22.0 1.00 11.1 1.11 1.00 11.1 1.11 1.00 100 11.0 1.00 100 11.0 1.00 200 22.0 1.00 200 22.0 1.00 500 55.0 1.00 50.0 5.50 1.00 500 55.0 1.00 Page 36 of 47 QC Report for Work Order (WO) -22J1703 Analyte % Rec RPD Limits RPD Max Result Source Cone Matrix Spike Dup -EPA 300.0 (cont.) QC Sample ID: BWJ1257-MSD2 Batch: BW11257 QC Source Sample: XXXXXXX-XX Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: mg/L Chloride 115 0.710 80 -120 20 11500 ND Fluoride 56.6 49.9 80 -120 20 566 ND QM-05 -The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The analytical batch was accepted based on the acceptable data provided by the Laboratory Control Sample(s) [LCS] and/or LCS Duplicates. Sulfate 99.3 0.502 80 -120 20 10900 1000 QC Sample ID: BW11470-MSD1 Batch: BW11470 QC Source Sample: XXXXXXX-XX Date Prepared: 10/31/2022 Date Analyzed: 11/01/2022 Units: mg/L Chloride 57.7 0.467 80 -120 20 2870 2290 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BW11470-MSD2 Batch: BW11470 QC Source Sample: XXXXXXX-XX Date Prepared: 10/31/2022 Date Analyzed: 11/01/2022 Units: mg/L Chloride 104 6.45 80 -120 20 11.5 ND QC Sample ID: BWK0078-MSD1 Batch: BWK0078 QC Source Sample: 2211703-06 Date Prepared: 11/02/2022 Date Analyzed: 11/02/2022 Units: mg/L Fluoride 88.7 0.00950 80 -120 20 5.79 1.36 QC Sample ID: BWK0078-MSD2 Batch: BWK0078 QC Source Sample: XXXXXXX-XX Date Prepared: 11/02/2022 Date Analyzed: 11/02/2022 Units: mg/L Fluoride 78.1 8.16 80 -120 20 0.966 0.098 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BWK0427-MSD1 Batch: BWK0427 QC Source Sample: 2211703-06 Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Chloride 96.9 0.402 80 -120 20 541 56.4 Sulfate 98.6 0.0406 80-120 20 4010 3520 CtF WO#: 22J1703 www.ChemtechFord.com Spk Value MRL DF 10000 1100 1.00 1000 110 1.00 10000 1100 1.00 1000 110 1.00 11.1 1.11 1.00 5.00 0.550 1.00 1.11 0.111 1.00 500 55.0 1.00 500 55.0 1.00 Page 37 of 47 Analyte QC Sample ID: BWJ1350-BLK1 Date Prepared: 11/02/2022 Ammonia as N QC Sample ID: BWJ1350-BS1 Date Prepared: 11/02/2022 Ammonia as N QC Sample ID: BWJ1350-MS1 Date Prepared: 11 /02/2022 Ammonia as N QC Sample ID: BWJ1350-MSD1 Date Prepared: 11/02/2022 Ammonia as N CtF WO#: 22J1703 www.ChemtechFord.com QC Report for Work Order (WO) -22J1703 % Rec RPD Limits RPD Max Result Source Cone Blank -EPA 350.1 Batch: BWJ1350 Date Analyzed: 11/02/2022 Units: mg/L ND LCS -EPA 350.1 Batch: BWJ1350 Date Analyzed: 11/02/2022 Units: mg/L 98.5 90 -110 0.985 Matrix Spike -EPA 350.1 Batch: BWJ1350 QC Source Sample: 2211703-06 Date Analyzed: 11/02/2022 Units: mg/L 106 80 -120 1.06 ND Matrix Spike Dup -EPA 350.1 Batch: BWJI 350 QC Source Sample: 2211703-06 Date Analyzed: 11/02/2022 Units: mg/L 118 11.1 80 -120 20 1.18 ND SpkValue MRL DF 0.0500 1.00 1.00 0.0500 1.00 1.00 0.0500 1.00 1.00 0.0500 1.00 Page 38 of 47 Analyte QC Sample ID: BWJl 130-BLKl Date Prepared: 10/24/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWJl 178-BLKJ Date Prepared: 10/25/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWJ1130-BS1 Date Prepared: 10/24/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWJl 178-BSl Date Prepared: 10/25/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWJ1130-MS1 Date Prepared: 10/24/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWJ1130-MS2 Date Prepared: 10/24/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWJl 178-MS 1 Date Prepared: 10/25/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWJ1178-MS2 Date Prepared: 10/25/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWJl 130-MSDl Date Prepared: 10/24/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWJl 130-MSD2 Date Prepared: 10/24/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWJl 178-MSDl Date Prepared: 10/25/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWJ1178-MSD2 Date Prepared: 10/25/2022 Nitrate + Nitrite, Total, as N CtF WO#: 22J1703 www.ChemtechFord.com QC Report for Work Order (WO) -22J1703 % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -EPA 353.2 Batch: BWJl 130 Date Analyzed: 10/24/2022 Units: mg/L ND 0.100 1.00 Batch: BWJl 178 Date Analyzed: 10/25/2022 Units: mg/L ND 0.100 1.00 LCS -EPA 353.2 Batch: BWJ1130 Date Analyzed: 10/24/2022 Units: mg/L 101 BO -120 2.02 2.00 0.100 1.00 Batch: BWJl 178 Date Analyzed: 10/25/2022 Units: mg/L 92.8 80 -120 1.86 2.00 0.100 1.00 Matrix Spike -EPA 353.2 Batch: BWJl 130 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/24/2022 Units: mg/L 114 80 -120 3.81 2,67 1.00 0.100 1.00 Batch: BWJl 130 QC Source Sample: 22Jl 703-06 Date Analyzed: 10/24/2022 Units: mg/L 88.1 80 -120 1.54 0.656 1.00 0.100 1.00 Batch: BWJl 178 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/25/2022 Units: mg/L 103 80 -120 1.03 ND 1.00 0.100 1.00 Batch: BWJl 178 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/25/2022 Units: mg/L 94.5 80 -120 1.07 0.122 1.00 0.100 1.00 Matrix Spike Dup -EPA 353.2 Batch: BWJl 130 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/24/2022 Units: mg/L 106 2.20 80 -120 20 3.73 2.67 1.00 0.100 1.00 Batch: BWJl 130 QC Source Sample: 22Jl 703-06 Date Analyzed: 10/24/2022 Units: mg/L 98.0 6.24 80 -120 20 1.64 0.656 1.00 0.100 1.00 Batch: BWJl 178 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/25/2022 Units: mg/L 116 11.9 80 -120 20 1.16 ND 1.00 0.100 1.00 Batch: BWJ1178 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/25/2022 Units: mg/L 99.7 4.76 80 -120 20 1.12 0.122 1.00 0.100 1.00 Page 39 of 47 QC Report for Work Order (WO) -22J1703 Analyte %Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -EPA 8260D /5030A QC Sample ID: BWJ1308-BLK1 Batch: BWJ1308 Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: ug/L Acetone ND 20.0 1,00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 QC Sample ID: BWJ1308-BLK2 Batch: BWJ1308 Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: ug/L Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 QC Sample ID: BWJ1308-BLK3 Batch: BWJ1308 Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: ug/L Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 QC Sample ID: BWJ1308-BLK4 Batch: BWJ1308 Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: ug/L Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 CtFWO#: 22J1703 www.ChemtechFord.com Page 40 of 47 QC Report for Work Order (WO) -22J1703 Analyte % Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 8260D /5030A (cont.) QC Sample ID: BWJ1308-BLK4 Batch: BWJ1308 Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: ug/L Xylenes, total ND 1.0 1.00 QC Sample ID: BWJ1308-BLK5 Batch: BWJ1308 Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: ug/L Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 LCS -EPA 8260D /5030A QC Sample ID: BWJ1308-BSI Batch: BWJ1308 Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: ug/L Acetone 86.4 70 -130 86.4 100 10.0 1.00 Benzene 93.3 70 -130 9.33 10.0 1.0 1.00 Carbon Tetrachloride 92.6 70 -130 9.26 10.0 1.0 1.00 Chloroform 93.4 70 -130 9.34 10.0 1.0 1.00 Chloromethane 77.8 70 -130 7.78 10.0 1.0 1.00 Methyl Ethyl Ketone 78.2 70 -130 78.2 100 10.0 1.00 Methylene Chloride 91.8 70 -130 9.18 10.0 1.0 1.00 Naphthalene 87.1 70 -130 8.71 10.0 1.0 1.00 Tetrahydrofuran 104 70 -130 10.4 10.0 1.0 1.00 Toluene 93.6 70 -130 9.36 10.0 1.0 1.00 Xylenes, total 96.4 70 -130 28.9 30.0 1.0 1.00 Matrix Spike -EPA 8260D /5030A QC Sample ID: BWJ1308-MS1 Batch: BWJ1308 QC Source Sample: 22Jl 703-06 Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: ug/L Acetone 83.8 70 -130 419 ND 500 50.0 1.00 Benzene 98.2 70 -130 49.1 ND 50.0 5.0 1.00 Carbon Tetrachloride 99.5 70 -130 49.8 ND 50.0 5.0 1.00 Chloroform 96.4 70 -130 48.2 ND 50.0 5.0 1.00 Chloromethane 86.4 70 -130 43.2 ND 50.0 5.0 1.00 Methyl Ethyl Ketone 77.5 70 -130 387 ND 500 50.0 1.00 Methylene Chloride 92.1 70 -130 46.0 ND 50.0 5.0 1.00 Naphthalene 84.9 70 -130 42.4 ND 50.0 5.0 1.00 Tetrahydrofuran 89.3 70 -130 44.6 ND 50.0 5.0 1.00 Toluene 98.7 70 -130 49.4 ND 50.0 5.0 1.00 Xylenes, total 97.4 70 -130 146 ND 150 5.0 1.00 Matrix Spike Dup -EPA 8260D /5030A QC Sample ID: BWJ1308-MSD1 Batch: BWJ1308 QC Source Sample: 2211703-06 Date Prepared: 10/26/2022 Date Analyzed: 10/26/2022 Units: ug/L Acetone 90.8 8.04 70 -130 20 454 ND 500 50.0 1.00 Benzene 94.9 3.42 70 -130 20 47.4 ND 50.0 5.0 1.00 Carbon Tetrachloride 95.5 4.10 70 -130 20 47.8 ND 50.0 5.0 1.00 CtF WO#: 22J1703 www.ChemtechFord.com Page 41 of 47 Analyte QC Sample ID: BWJ1308-MSD1 Date Prepared: 10/26/2022 Chloroform Chloromethane Methyl Ethyl Ketone Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total CtF WO#: 22J1703 www.ChemtechFord.com QC Report for Work Order (WO) -22J1703 % Rec RPO Limits RPO Max Result Source Cone Matrix Spike Dup -EPA 8260D /5030A (cont.) Batch: BWJ1308 QC Source Sample: 22J 1703-06 Date Analyzed: 10/26/2022 Units: ug/L 95.0 1.46 70 -130 20 47.5 ND 89.0 2.96 70 -130 20 44.5 ND 85.3 9.60 70 -130 20 426 ND 94.3 2.36 70 -130 20 47.2 ND 91.2 7.16 70 -130 20 45.6 ND 104 15.1 70 -130 20 52.0 ND 96.2 2.57 70 -130 20 48.1 ND 98.5 1.19 70 -130 20 148 ND SpkValue MRL OF 50.0 5.0 1.00 50.0 5.0 1.00 500 50.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 150 5.0 1.00 Page 42 of 47 Analyte QC Sample ID: BWJI077-BLKI Date Prepared: I 0/2 I /2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) QC Sample ID: BWJI 142-BLKI Date Prepared: 10/24/2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) QC Sample ID: BWJI077-DUPI Date Prepared: I 0/21 /2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Alkalinity -Total (as CaCO3) QC Sample ID: BWJl 142-DUPI Date Prepared: 10/24/2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Alkalinity -Total (as CaCO3) QC Sample ID: BWJl077-BSI Date Prepared: 10/21/2022 Alkalinity -Total (as CaCO3) QC Sample ID: BWJll42-BSI Date Prepared: I 0/24/2022 Alkalinity -Total (as CaCO3) CtF WO#: 22J1703 www.ChemtechFord.com QC Report for Work Order (WO) -22J1703 % Rec RPO Limits RPO Max Result Source Cone Blank -SM 2320 B Batch: BWJI077 Date Analyzed: 10/21 /2022 Units: mg/L ND ND Batch: BWJI 142 Date Analyzed: I 0/24/2022 Units: mg/L ND ND Duplicate -SM 2320 B Batch: BWJI077 QC Source Sample: XXXXXXX-XX Date Analyzed: I 0/21 /2022 Units: mg/L 0.100 20 199 199 20 ND ND 0.100 20 199 199 Batch: BWJI 142 QC Source Sample: 2211703-06 Date Analyzed: 10/25/2022 Units: mg/L 0.477 20 293 294 20 ND ND 0.477 20 293 294 LCS -SM 2320 B Batch: BWJI077 Date Analyzed: I 0/21 /2022 Units: mg/L 98.5 90 -110 232 Batch: BWJI 142 Date Analyzed: I 0/24/2022 Units: mg/L 97.1 90 -110 229 Spk Value MRL OF 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 1.0 1.00 236 1.0 1.00 236 1.0 1.00 Page 43 of 47 Analyte QC Sample ID: BWJ1064-BLK1 Date Prepared: 10/21/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ1065-BLK1 Date Prepared: 10/21/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ1086-BLK1 Date Prepared: 10/2 l /2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ1064-DUP1 Date Prepared: 10/21/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJl 064-DUP2 Date Prepared: 10/2 l /2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ1065-DUP1 Date Prepared: 10/2 l /2022 Total Dissolved Solids (TDS) QC Sample ID: BWJl 065-DUP2 Date Prepared: 10/21/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ1086-DUP1 Date Prepared: 10/21/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ1086-DUP2 Date Prepared: 10/2 l /2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ1064-BS1 Date Prepared: 10/21/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ1065-BS1 Date Prepared: 10/21/2022 Total Dissolved Solids (TDS) QC Sample ID: BWJ1086-BS1 Date Prepared: 10/21/2022 Total Dissolved Solids (TDS) CtF WO#: 22J1703 www.ChemtechFord.com QC Report for Work Order (WO) -22J1703 %Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -SM 2540 C Batch: BWJ1064 Date Analyzed: 10/24/2022 Units: mg/L ND 10 1.00 Batch: BWJ1065 Date Analyzed: 10/24/2022 Units: mg/L ND 20 1.00 Batch: BWJ1086 Date Analyzed: 10/24/2022 Units: mg/L ND 20 1.00 Duplicate -SM 2540 C Batch: BWJ1064 QC Source Sample: 2211703-06 Date Analyzed: 10/24/2022 Units: mg/L 2 10 5180 5270 20 1.00 Batch: BWJ1064 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/24/2022 Units: mg/L 0.08 10 4720 4720 20 1.00 Batch: BWJ1065 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/24/2022 Units: mg/L 2 10 244 248 20 1.00 Batch: BWJ1065 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/24/2022 Units: mg/L 0.07 10 5670 5660 20 1.00 Batch: BWJ1086 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/24/2022 Units: mg/L 0.9 10 864 872 20 1.00 Batch: BWJ1086 QC Source Sample: XXXXXXX-XX Date Analyzed: 10/24/2022 Units: mg/L 0.2 10 9380 9400 100 1.00 LCS -SM 2540 C Batch: BWJ1064 Date Analyzed: 10/24/2022 Units: mg/L 98 90 -110 392 400 20 1.00 Batch: BWJ1065 Date Analyzed: 10/24/2022 Units: mg/L 101 90 -110 404 400 20 1.00 Batch: BWJ1086 Date Analyzed: 10/24/2022 Units: mg/L 95 90-110 380 400 20 1.00 Page 44 of 47 Surrogates Report for Work Order (WO) -22J1703 QCID Analyte BWJ1308-BLK4 1,2-Dichloroethane-d4 BWJ 1308-BLK2 1,2-Dichloroethane-d4 BWJ1308-BLK5 1,2-Dichloroethane-d4 BWJ1308-BLK3 1,2-Dichloroethane-d4 BWJ1308-BLK1 1,2-Dichloroethane-d4 BWJ1308-BLK1 4-Bromofluorobenzene BWJ1308-BLK2 4-Bromofluorobenzene BWJ 1308-BLK4 4-Bromofluorobenzene BWJ1308-BLK5 4-Bromofluorobenzene BWJ1308-BLK3 4-Bromofluorobenzene BWJ1308-BLK2 Toluene-dB BWJ1308-BLK3 Toluene-dB BWJ 1308-BLK 1 Toluene-dB BWJ 1308-BLK5 Toluene-dB BWJ1308-BLK4 Toluene-dB BWJ 1308-BS 1 1,2-Dichloroethane-d4 BWJ1308-8S1 4-Bromofluorobenzene BWJ1308-8S1 Toluene-dB BWJ1308-MS1 1,2-Dichloroethane-d4 BWJ1308-MS1 4-Bromofluorobenzene BWJ1308-MS1 Toluene-dB BWJ1308-MSD1 1,2-Dichloroethane-d4 BWJ1308-MSD1 4-Bromofluorobenzene BWJ1308-MSD1 Toluene-dB CtF WO#: 22J1703 www.ChemtechFord.com % Rec LCL UCL Result Blank -EPA 8260D /5030A 101 64.2 126 10.1 102 64.2 126 10.2 102 64.2 126 10.2 102 64.2 126 10.2 97.7 64.2 126 9.77 98.2 71.4 125 9.82 97.1 71.4 125 9.71 93.9 71.4 125 9.39 94.6 71.4 125 9.46 95.3 71.4 125 9.53 100 63.2 129 10.0 101 63.2 129 10.1 98.1 63.2 129 9.81 100 63.2 129 10.0 100 63.2 129 10.0 LCS -EPA 8260D /5030A 94.6 64.2 126 9.46 100 71.4 125 10.0 99.2 63.2 129 9.92 Matrix Spike -EPA 8260D /5030A 94.2 64.2 126 47.1 98.3 71.4 125 49.2 100 63.2 129 50.0 Matrix Spike Dup -EPA 8260D /5030A 97.0 64.2 126 48.5 96.0 71.4 125 48.0 100 63.2 129 50.0 SpkValue Batch DF 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 10.0 BWJ1308 1.00 50.0 BWJ1308 1.00 50.0 BWJ1308 1.00 50.0 BWJ1308 1.00 50.0 BWJ1308 1.00 50.0 BWJ1308 1.00 50.0 BWJ1308 1.00 Page 45 of 47 Surrogate Recoveries (Field Samples) LabNumber Analyte 8260 Low Level Volatiles 22J1703-01 4-Bromofluorobenzene 22J1703-01 Toluene-dB 22J1703-01 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22J 1703-02 1,2-Dichloroethane-d4 22J1703-02 22J1703-02 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22J1703-03 4-Bromofluorobenzene 22J1703-03 22J1703-03 Toluene-dB 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22J1703-04 4-Bromofluorobenzene 22J1703-04 22J1703-04 Toluene-dB 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22J1703-05 1,2-Dichloroethane-d4 22J1703-05 22J1703-05 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22J1703-06 Toluene-dB 22J1703-06 22J1703-06 4-Bromofluorobenzene 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22J1703-07 1,2-Dichloroethane-d4 22J1703-07 22J1703-07 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22J1703-08 Toluene-dB 22J1703-08 1,2-Dichloroethane-d4 CtF WO#: 22J1703 www.ChemtechFord.com Result 9.51 10.0 9.30 9.71 9.60 9.98 9.84 10.0 9.99 9.66 10.0 9.97 10.0 9.87 10.0 9.99 9.44 9.87 10.3 9.60 10.2 10.1 9.92 SpkLvl 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 %Rec 95.1 100 93.0 97.1 96.0 99.8 98.4 100 99.9 96.6 100 99.7 100 98.7 100 99.9 94.4 98.7 103 96.0 102 101 99.2 LCL UCL Qualifier 71.4 125 63.2 129 64.2 126 64.2 126 71.4 125 63.2 129 71.4 125 63.2 129 64.2 126 71.4 125 63.2 129 64.2 126 64.2 126 71.4 125 63.2 129 63.2 129 71.4 125 64.2 126 64.2 126 71.4 125 63.2 129 63.2 129 64.2 126 Page 46 of 47 22J1703-0B 4-Bromofluorobenzene 8260 Low Level Volatiles 22J1703-09 Toluene-dB 22J1703-09 22J1703-09 1,2-Dichloroethane-d4 4-Bromofluorobenzene 8260 Low Level Volatiles 22J 1703-1 O 1,2-Dichloroethane-d4 22J1703-10 22J1703-10 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22J 1703-11 Toluene-dB 22J1703-11 22J1703-11 1,2-Dichloroethane-d4 4-Bromofluorobenzene CtF WO#: 22J1703 www.ChemtechFord.com 9.61 10.0 10.4 9.59 10.1 9.43 10.1 10.0 10.2 9.62 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 96.1 100 104 95.9 101 94.3 101 100 102 96.2 71.4 125 63.2 129 64.2 126 71.4 125 64.2 126 71.4 125 63.2 129 63.2 129 64.2 126 71.4 125 Page 47 of 47 9632 South 500 West CHEMTECH·FORD L,\ ~ 1J R,\TO~ IES Amended 12/21/2022 Work Order: 22K0334 Project: 4th Quarter Ground Water 2022 Energy Fuels Resources, Inc. Attn: Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Client Service Contact: 801.262. 7299 The analyses presented on this report were performed in accordance with the National Environmental Laboratory Accreditation Program (NELAP) unless noted in the comments, flags, or case narrative. If the report is to be used for regulatory compliance, it should be presented in its entirety, and not be altered. Approved By: ~~ Melissa Connolly, Project Manager Sandy, Utah 84070 801 .262.7299 Main 866.792.0093 Fax Serving the lntermountain West since 1953 www.ChemtechFord.com Page 1 of 39 CHEMTECH-FORD lABOl!AfORIES Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Energy Fuels Resources, Inc. Project: 4th Quarter Ground Water 2022 Project Manager: Tanner Holliday Laboratory ID 22K0334-01 22K0334-02 22K0334-03 22K0334-04 22K0334-05 22K0334-06 22K0334-07 22K0334-08 22K0334-09 22K0334-10 Sample Name MW-35_ 10312022 MW-70_ 10312022 MW-20_ 11012022 MW-23_ 11012022 MW-37 _ 11012022 MW-38_ 11012022 TW4-24_ 11012022 MW-24_ 11022022 MW-24A_ 11022022 Trip Blank Amended Work Order Report Narrative Amendment Notes The Mercury result for 22K0334-02 has been updated due to a laboratory data entry error. Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions There are no corrective actions associated with this work order. Page 2 of 39 CHEMTECH-FORD lA80RArORIES Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Amended Certificate of Analysis Amended Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations ND= Not detected at the corresponding Minimum Reporting Limit (MRL), PO#: Receipt: 11/3/22 12:10@ -3.1 °C Date Reported: 12/21/2022 Project Name: 4th Quarter Ground Water 2022 I mg/L = one milligram per liter or I mg/kg = one milligram per kilogram = I part per million. I ug/L = one microgram per liter or I ug/kg = one microgram per kilogram = I part per billion. I ng/L = one nanogram per liter or I ng/kg = one nanogram per kilogram = I part per trillion. Proiect Name: 4th Quarter Ground Water 2022 www.ChemtechFord.com CtF WO#: 22K0334 Page 22 of 39 American West Analytical Laboratories 463 W. 3600 S, Salt Lake City, UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 .1-~ Fax# (801) 263-8687 Email awal@awel~abs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 8. Hwy. 191 Blanding, UT 84511 Contact Tanner HoWday Phone#: (435) 678-2221 Cell#: Email: thoWday@eneqyfaelll.com; KWelnel@:enerlYfttela.com Projecl Name: 4th Quarter Ground Water 2022 Project#: PO#: Sampler Name: Tanner HoWday 22K0334 SamJ)le ID: Date Sampled IIIW-35_10312022 10/31/2022 2 · IIIW-70 10312022 10/31/2022 3 , IIIW-20_11012022 11/1/2022 IIIW-23_11012022 11/1/2022 IIIW-37 _11012022 11/1/2022 IIIW-38_11012022 11/1/2022 TW4-24_11012022 11/1/2022 8 IIIW-24 11022022 11/2/2022 IIIW-24A_l1022022 11/2/2022 ) Trip Blank 10/31/2022 I ! Rollnqulahodby: :1 If,{/~ Date: Slgnellfl'O -I"""..... • 1112/2022 V Tlma: PrtntName: Tannner Holllday 113! Rollnqulahed by: Date: Signature Tlma: PrtntNam■: Rellnqlllahed by: Date: Signature Time: Print Name: Raltnqutaned Dy: Data: Sklnature Tlme: Prtnt Name: v'?S:. \1. \~7 'i1'/ cs qz~-1 ulY) CHAIN OF CUSTODY All enelyala wUI be condueted using NELAP aCCfedlted methods and all data will be reported ualng AWAL'a etandard analyte lleta and reporting llmlls (POL) uni ... apeclOcally requealed olhorMsa on 1h11 Chain ol Cuollldy and/or aHeched documentation. AWAL Lab Sample Set# Page 1 of 1 I QC Level: I Turn Around Time: Unleaa other arrangement& have been made, I°"'""' I algned r"l)Ofla ~• be emailed by 5:00 pm on 3 Standard the day they ere due. X Include EDD: Laboratory Use Only 0 LOCUS UPLOAD ::. "' EXCEL Sampl•Wwo u oi, "° X Field FIitered For: :c Dlnolved Metala , czorhenddollvo,od -::. .... i:: 2 blonte It) :l "' ::. <'I ,0 .,j' For Compllance With: 3 Tomp«•turo -il•c ~ z p. □ NELAP \ c:i ,; ci' s-c:, i;.. N □ RCRA <'I " > □ CWA 4 ROG<!lvod Brok....,_ool,,lng \ c:i ~ u □ SOWA (lmpropel1y Saoled) c:, c::i :i y ~ \ :::;-"> iii' c:, 0 □ ELAP/A2LA ci .. ~ u ci' □ NLLAP 0 c:, U) ~ It) c:, ~ -; .: \ □ Non-Compliance 5 P,opo,ty P,-,,ad "> c:, u ¢ (Y/ N ~ .. It) ~ ... □ Other: 0 ~ D '0 oi, G' Clloc:kada!b9nch ~ ~ 0 G' A :a u <C D c:, ., >< Cl § c:, :a u IC y N C :s C'l c:, "' ~ "Cl ,; ,; i <'I ~ .. 0 It) It) D ID U) ~ Known Hazards 6 Received Wl!hln ::; lz: ~ ~ IQ .e: 0 3! -~ -j ,,; z j Holdil,gT1mes Time 0 a. s C'l () !Ill ,Q ,( & C) E ~ Q :a II N 0 if Samoled .. .,i lz: ... 0 .!! Sample Comments 1345 7 w X X X X X X X X X X A?(~ 1 -l'L')D 1345 7 w X X X X X X X X X X tJ -\rl 31. jcOCT-W•: rv\ -1'2.-1lb 1 ~! on Outer Package 1200 7 w X X X X X X X X X X Y N NA 1245 7 w X X X X X X X X X X vJ(?,) -1?.o 3 2 c7kon on Outer Paciu,g. Y N NA 1305 7 w X X X X X X X X X X -10 vv R J 3 Prwent on Sample fl 1230 7 w X X X X X X X X X X y N A I 1330 7 w X X X X X X X X X X tPl\Jf-\l 4 Unbrokan on Sample e: y N 645 7 w X X X X X X X X X X 700 7 w X X X X X X X X X X Olacrepanolea s.twaen Sample 1345 3 w X y N I Labela and COC Reco~ ) I ~ R-,.,a<I b1// SJanetvra /~ Dale:, l /3 ''t'l..,, Speelal Instructions: pa ~{~t} Tim•j l'l_: i n Sam ple containers for metals were field filtered. See the Racelved by: Date: Analytical Scope of Work for Reporting Limits and VOC analyte S'9noture list. Time: Prln1Namo: :--Roc<llvod by; Sample Receipt Conditions: ~•cl Containers Slgn•~iro J1sustody Seals Present ~adspace Present (VOC) ,-- PrlnlN111rne: JA'c:onlillnierJ lnlact COC Included ( ) Temperature Blank :-RaceNedby: ~oc and t..,bels M,1\Ch M(OC Complete J...l•Recelvt<t wi~).old ~noluro [.;rSufficient Sample Volume Cht<kod by: , '/ -0'eceived on Ice Page 23 of 39 P,1n1Namo: QC Report for Work Order (WO) -22K0334 Analyte %Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 200.7 QC Sample ID: BWK0365-BLK1 Batch: BWK0365 Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Calcium, Dissolved ND 0.2 1.00 Iron, Dissolved ND 0.03 1.00 Magnesium, Dissolved ND 0.2 1.00 Potassium, Dissolved ND 0.5 1.00 Sodium, Dissolved ND 0.5 1.00 Tin, Dissolved ND 0.10 1.00 LCS -EPA 200. 7 QC Sample ID: BWK0365-BS1 Batch: BWK0365 Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Calcium, Dissolved 97.9 85 -115 10.0 10.2 0.2 1.00 Iron, Dissolved 104 85 -115 0.207 0.200 0.02 1.00 Magnesium, Dissolved 99.2 85 -115 10.1 10.2 0.2 1.00 Potassium, Dissolved 98.4 85 -115 9.8 10.0 0.5 1.00 Sodium, Dissolved 96.8 85 -115 9.7 10.0 0.5 1.00 Tin, Dissolved 99.3 85 -155 0.20 0.201 0.02 1.00 Matrix Spike -EPA 200.7 QC Sample ID: BWK0365-MS1 Batch: BWK0365 QC Source Sample: XXXXXXX-XX Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Calcium, Dissolved 99.4 70 -130 53.8 43.7 10.2 0.2 1.00 Iron, Dissolved 107 70 -130 0.214 ND 0.200 0.02 1.00 Magnesium, Dissolved 101 70 -130 29.0 18.8 10.2 0.2 1.00 Potassium, Dissolved 98.8 70 -130 11.9 2.0 10.0 0.5 1.00 Sodium, Dissolved 95.3 70 -130 45.0 35.5 10.0 0.5 1.00 Tin, Dissolved 103 70 -130 0.21 ND 0.201 0.02 1.00 QC Sample ID: BWK0365-MS2 Batch: BWK0365 QC Source Sample: 22K0334-0l Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Calcium, Dissolved 162 70 -130 512 496 10.2 0.2 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Iron, Dissolved 110 70 -130 0.428 0.208 0.200 0.02 1.00 Magnesium, Dissolved 125 70 -130 171 158 10.2 0.2 1.00 Potassium, Dissolved 106 70 -130 21.4 10.8 10.0 0.5 1.00 Sodium, Dissolved 105 70 -130 372 361 10.0 0.5 1.00 Tin, Dissolved 107 70 -130 0.23 0.01 0.201 0.02 1.00 Matrix Spike Dup -EPA 200.7 QC Sample ID: BWK0365-MSD1 Batch: BWK0365 QC Source Sample: XXXXXXX-XX Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Calcium, Dissolved 106 1.24 70 -130 20 54.5 43.7 10.2 0.2 1.00 Iron, Dissolved 103 3.81 70 -130 20 0.206 ND 0.200 0.02 1.00 Magnesium, Dissolved 106 1.66 70 -130 20 29.5 18.8 10.2 0.2 1.00 Potassium, Dissolved 103 3.10 70 -130 20 12.3 2.0 10.0 0.5 1.00 Sodium, Dissolved 102 1.40 70 -130 20 45.7 35.5 10.0 0.5 1.00 Tin, Dissolved 103 0.627 70 -130 20 0.21 ND 0.201 0.02 1.00 QC Sample ID: BWK0365-MSD2 Batch: BWK0365 QC Source Sample: 22K0334-0l Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: mg/L Calcium, Dissolved 83.9 1.57 70 -130 20 504 496 10.2 0.2 1.00 Iron, Dissolved 112 0.954 70 -130 20 0.432 0.208 0.200 0.02 1.00 CtF WO#: 22K0334 www. Chem tech Ford. com Page 24 of 39 Analyte QC Sample ID: BWK0365-MSD2 Date Prepared: 11 /08/2022 Magnesium, Dissolved Potassium, Dissolved QC Report for Work Order (WO) -22K0334 % Rec RPO Limits RPO Max Result Source Cone Matrix Spike Dup -EPA 200.7 (cont.) Batch: BWK0365 QC Source Sample: 22K0334-0 I Date Analyzed: 11/08/2022 98.6 106 1.57 0.195 70 -130 70 -130 20 20 168 21.3 Units: mg/L 158 10.8 Sodium, Dissolved 66.7 1.05 70 -130 20 368 361 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 limes or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Tin .Dissolved 102 4.12 70-130 20 0.22 0.01 CtF WO#: 22K0334 www.ChemtechFord.com SpkValue 10.2 10.0 10.0 0.201 MRL 0.2 0.5 0.5 0.02 OF 1.00 1.00 1.00 1.00 Page 25 of 39 QC Report for Work Order (WO) -22K0334 Analyte % Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -EPA 200.8 QC Sample ID: BWK.0590-BLKl Batch: BWK0590 Date Prepared: 11/14/2022 Date Analyzed: 11 /14/2022 Units: mg/L Arsenic, Dissolved ND 0.0050 1.00 Beryllium, Dissolved ND 0.0005 1.00 Cadmium, Dissolved ND 0.0005 1.00 Chromium, Dissolved ND 0.0250 1.00 Cobalt, Dissolved ND 0.010 1.00 Copper, Dissolved ND 0.0100 1.00 Lead, Dissolved ND 0.0010 1.00 Manganese, Dissolved ND 0.0100 1.00 Molybdenum, Dissolved ND 0.0100 1.00 Nickel, Dissolved ND 0.0200 1.00 Selenium, Dissolved ND 0.0050 1.00 Silver, Dissolved ND 0.010 1.00 Thallium, Dissolved ND 0.0005 1.00 Uranium, Dissolved ND 0.0003 1.00 Vanadium, Dissolved ND 0.0150 1.00 Zinc, Dissolved ND 0.0100 1.00 LCS -EPA 200.8 QC Sample ID: BWK0590-BS1 Batch: BWK0590 Date Prepared: 11/14/2022 Date Analyzed: 11 /14/2022 Units: mg/L Arsenic, Dissolved 105 85 -115 0.042 0.0400 0.0005 1.00 Beryllium, Dissolved 109 85 -115 0.044 0.0400 0.0005 1.00 Cadmium, Dissolved 106 85 -115 0.042 0.0400 0.0002 1.00 Chromium, Dissolved 106 85 -115 0.043 0.0400 0.0005 1.00 Cobalt, Dissolved 107 85 -115 0.043 0.D400 0.0005 1.00 Copper, Dissolved 104 85 -115 0.041 0.0400 0.0010 1.00 Lead , Dissolved 106 85 -115 0.042 0.0400 0.0005 1.00 Manganese, Dissolved 105 85 -115 0.042 0.D400 0.0005 1.00 Molybdenum, Dissolved 107 85 -115 0.043 0.0400 0.0005 1.00 Nickel, Dissolved 103 85 -115 0.0413 0.0400 0.0005 1.00 Selenium, Dissolved 104 85 -115 0.042 0.0400 0.0005 1.00 Silver, Dissolved 99.1 85 -115 0.040 0.0400 0.0005 1.00 Thallium, Dissolved 111 85 -115 0.044 0.0400 0.0002 1.00 Uranium, Dissolved 108 85 -115 0.043 0.0400 0.0003 1.00 Vanadium, Dissolved 108 85 -115 0.043 0.0400 0.0005 1.00 Zinc, Dissolved 103 85 -115 0.041 0.0400 0.0100 1.00 Matrix Spike -EPA 200.8 QC Sample ID: BWK0590-MS1 Batch: BWK0590 QC Source Sample: 22K0334-0 l Date Prepared: 11/14/2022 Date Analyzed: 11/14/2022 Units: mg/L Arsenic, Dissolved 117 70 -130 0.048 0.0009 0.0400 0.0005 1.00 Beryllium, Dissolved 107 70 -130 0.043 ND 0.0400 0.0005 1.00 Cadmium, Dissolved 103 70 -130 0.041 0.00004 0.0400 0.0002 1.00 Chromium, Dissolved 102 70 -130 0.047 0.006 0.0400 0.0005 1.00 Cobalt, Dissolved 98.6 70 -130 0.043 0.003 0.0400 0.0005 1.00 Copper, Dissolved 90.3 70 -130 0.042 0.006 0.Q400 0.0010 1.00 Lead, Dissolved 101 70 -130 0.040 ND 0.0400 0.0005 1.00 Manganese, Dissolved 100 70 -130 0.303 0.263 0.0400 0.0005 1.00 Molybdenum, Dissolved 112 70 -130 0.045 0.0006 0.0400 0.0005 1.00 Nickel, Dissolved 91 .2 75 -125 0.0483 0.0118 0.0400 0.0005 1.00 Selenium, Dissolved 125 70 -130 0.062 0.012 0.0400 0.0005 1.00 CtF WO#: 22K0334 www.ChemtechFord.com Page 26 of 39 QC Report for Work Order (WO) -22K0334 Analyte %Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Matrix Spike -EPA 200.8 (cont.) QC Sample ID: BWK.0590-MSI Batch: BWK.0590 QC Source Sample: 22K0334-01 Date Prepared: 11/14/2022 Date Analyzed: 11/14/2022 Units: mg/L Silver, Dissolved 89.3 70 -130 0.036 ND 0.0400 0.0005 1.00 Thallium, Dissolved 104 70 -130 0.042 0.0004 0.0400 0.0002 1.00 Uranium, Dissolved 110 70 -130 0.066 0.022 0.0400 0.0003 1.00 Vanadium, Dissolved 107 70 -130 0.044 0.002 0.0400 0.0005 1.00 Zinc, Dissolved 92.6 70 -130 0.039 0.002 0.0400 0.0100 1.00 QC Sample ID: BWK0590-MS2 Batch: BWK.0590 QC Source Sample: XXXXXXX-XX Date Prepared: 11/14/2022 Date Analyzed: 11/14/2022 Units: mg/L Arsenic, Dissolved 107 70 -130 0.044 0.001 0.0400 0.0005 1.00 Beryllium, Dissolved 106 70 -130 0.042 ND 0.0400 0.0005 1.00 Cadmium, Dissolved 102 70 -130 0.041 0.0003 0.0400 0.0002 1.00 Chromium, Dissolved 103 70 -130 0.042 0.0007 0.0400 0.0005 1.00 Cobalt, Dissolved 99.0 70 -130 0.040 0.0004 0.0400 0.0005 1.00 Copper, Dissolved 98.5 70 -130 0.042 0.003 0.0400 0.0010 1.00 Lead , Dissolved 101 70 -130 0.048 0.008 0.0400 0.0005 1.00 Manganese, Dissolved 98.0 70 -130 0.101 0.062 0.0400 0.0005 1.00 Molybdenum, Dissolved 108 70 -130 0.048 0.004 0.0400 0.0005 1.00 Nickel, Dissolved 98.1 75 -125 0.0408 0.0016 0.0400 0.0005 1.00 Selenium, Dissolved 106 70 -130 0.043 0.0004 0.0400 0.0005 1.00 Silver, Dissolved 94.9 70 -130 0.038 ND 0.0400 0.0005 1.00 Thallium, Dissolved 102 70 -130 0.041 ND 0.0400 0.0002 1.00 Uranium, Dissolved 103 70 -130 0.041 0.0002 0.0400 0.0003 1.00 Vanadium, Dissolved 107 70 -130 0.043 0.0002 0.0400 0.0005 1.00 Zinc, Dissolved 97.3 70 -130 0.081 0.042 0.0400 0.0100 1.00 Matrix Spike Dup -EPA 200.8 QC Sample ID: BWK0590-MSDI Batch: BWK0590 QC Source Sample: 22K0334-0I Date Prepared: 11 /14/2022 Date Analyzed: 11/14/2022 Units: mg/L Arsenic, Dissolved 114 2.29 70 -130 20 0.046 0.0009 0.0400 0.0005 1.00 Beryllium, Dissolved 93.9 13.4 70 -130 20 0.038 ND 0.0400 0.0005 1.00 Cadmium, Dissolved 98.7 3.73 70 -130 20 0.040 0.00004 0.0400 0.0002 1.00 Chromium, Dissolved 96.9 4.51 70 -130 20 0.045 0.006 0.0400 0.0005 1.00 Cobalt, Dissolved 94.3 4.16 70 -130 20 0.041 0.003 0.0400 0.0005 1.00 Copper, Dissolved 90.3 0.00239 70 -130 20 0.042 0.006 0.0400 0.0010 1.00 Lead, Dissolved 93.5 7.86 70 -130 20 0.037 ND 0.0400 0.0005 1.00 Manganese, Dissolved 110 1.32 70 -130 20 0.307 0.263 0.0400 0.0005 1.00 Molybdenum, Dissolved 109 3.14 70 -130 20 0.044 0.0006 0.0400 0.0005 1.00 Nickel, Dissolved 92.4 0.966 75 -125 20 0.0488 0.0118 0.0400 0.0005 1.00 Selenium, Dissolved 127 0.823 70 -130 20 0.063 0.012 0.0400 0.0005 1.00 Silver, Dissolved 82.3 8.21 70 -130 20 0.033 ND 0.0400 0.0005 1.00 Thallium, Dissolved 95.2 8.42 70 -130 20 0.038 0.0004 0.0400 0.0002 1.00 Uranium, Dissolved 101 5.06 70 -130 200 0.063 0.022 0.0400 0.0003 1.00 vanadium, Dissolved 104 2.18 70 -130 20 0.044 0.002 0.0400 0.0005 1.00 ~inc, Dissolved 88.7 3.97 70 -130 20 0.038 0.002 0.0400 0.0100 1.00 • :tF WO#: 22K0334 'WW. ChemtechFord. com Page 27 of 39 Analyte QC Sample ID: BWK0461-BLK1 Date Prepared: 11/10/2022 Mercury, Dissolved QC Sample ID: BWK0461-BS1 Date Prepared: 11/10/2022 Mercury, Dissolved QC Sample ID: BWK0461-MS1 Date Prepared: 11/10/2022 Mercury, Dissolved QC Sample ID: BWK0461-MSD1 Date Prepared: 11/10/2022 Mercury, Dissolved CtF WO#: 22K0334 www.ChemtechFord.com QC Report for Work Order (WO) -22K0334 % Rec RPO Limits RPO Max Result Source Cone Blank -EPA 245.1 Batch: BWK0461 Date Analyzed: 11/10/2022 Units: mg/L ND LCS -EPA 245.1 Batch: BWK0461 Date Analyzed: 11/10/2022 Units: mg/L 107 85 -115 0.00536 Matrix Spike -EPA 245.1 Batch: BWK0461 QC Source Sample: 22K0334-0l Date Analyzed: 11/10/2022 Units: mg/L 103 75 -125 0.00516 ND Matrix Spike Dup -EPA 245.1 Batch: BWK0461 QC Source Sample: 22K0334-01 Date Analyzed: 11/10/2022 Units: mg/L 108 4.94 75 -125 20 0.00542 ND Spk Value MRL OF 0.00050 1.00 0.00500 0.00015 1.00 0.00500 0.00015 1.00 0.00500 0.00015 1.00 Page 28 of 39 QC Report for Work Order (WO) -22K0334 Analyte % Rec RPO Limits RPO Max Result Source Cone Blank -EPA 300.0 QC Sample ID: BWK0546-BLK1 Batch: BWK0546 Date Prepared: 11/11/2022 Date Analyzed: 11/14/2022 Units: mg/L Chloride ND Fluoride ND Sulfate ND QC Sample ID: BWK0890-BLK1 Batch: BWK0890 Date Prepared: 11/18/2022 Date Analyzed: 11/19/2022 Units: mg/L Sulfate ND LCS -EPA 300.0 QC Sample ID: BWK0546-BSI Batch: BWK0546 Date Prepared: 11/11/2022 Date Analyzed: 11/14/2022 Units: mg/L Chloride 95.6 90 -110 47.8 Fluoride 93.2 90 -110 4.66 Sulfate 92.6 90 -110 46.3 QC Sample ID: BWK0890-BSI Batch: BWK0890 Date Prepared: 11/18/2022 Date Analyzed: 11/19/2022 Units: mg/L Sulfate 99.5 90 -110 49.7 Matrix Spike -EPA 300.0 QC Sample ID: BWK0546-MS1 Batch: BWK0546 QC Source Sample: 22K0334-0l Date Prepared: 11/11/2022 Date Analyzed: 11/14/2022 Units: mg/L Chloride 76.3 80 -120 442 60.6 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD . The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO . Fluoride 89.0 80 -120 44.5 ND Sulfate 103 80 -120 2650 2130 QC Sample ID: BWK0546-MS2 Batch: BWK0546 QC Source Sample: XXXXXXX-XX Date Prepared: 11/11/2022 Date Analyzed: 11114/2022 Units: mg/L Chloride 77.8 80 -120 461 71.9 Fluoride 92.6 80 -120 46.3 ND Sulfate 98.4 80 -120 1630 1140 QC Sample ID: BWK0890-MS1 Batch: B WK0890 QC Source Sample: XXXXXXX-XX Date Prepared: 11/18/2022 Date Analyzed: 1 I /19/2022 Units: mg/L Sulfate 106 80 -120 462 356 Matrix Spike Dup -EPA 300.0 QC Sample ID: BWK0546-MSD1 Batch: BWK0546 QC Source Sample: 22K0334-0l Date Prepared: 11/11/2022 Date Analyzed: 11/14/2022 Units: mg/L Chloride 75.4 1.05 80 -120 20 437 60.6 QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. Fluoride Sulfate QC Sample ID: BWK0546-MSD2 Date Prepared: 11/11/2022 Chloride Fluoride Sulfate CtF WO#: 22K0334 www.ChemtechFord.com 92.3 3.65 80 -120 20 46.2 ND 103 0.00711 80 -120 20 2650 2130 Batch: B WK0546 QC Source Sample: XXXXXXX-XX Date Analyzed: 11/15/2022 Units: mg/L 77.5 0.337 80 -120 20 460 71.9 92.4 0.166 80 -120 20 46.2 ND 98.2 0.0530 80 -120 20 1630 1140 Spk Value MRL OF 1.00 1.00 0.100 1.00 1.00 1.00 1.00 1.00 50.0 1.00 1.00 5.00 0.100 1.00 50.0 1.00 1.00 50.0 1.00 1.00 500 55.0 1.00 50.0 5.50 1.00 500 55.0 1.00 500 55.0 1.00 50.0 5.50 1.00 500 55.0 1.00 100 11.0 1.00 500 55.0 1.00 50.0 5.50 1.00 500 55.0 1.00 500 55.0 1.00 50.0 5.50 1.00 500 55.0 1.00 Page 29 of 39 QC Report for Work Order (WO) -22K0334 Analyte %Rec RPD Limits RPDMax Result Source Cone Matrix Spike Dup -EPA 300.0 (cont.) QC Sample ID: BWK.0890-MSDl Batc;h: BWK.0890 QC Source Sample: XXXXXXX-XX Date Prepared: 11/18/2022 DateAnalyzed: 11/19/2022 Units: Sulfate 153 9.76 80 -120 20 509 356 OM-12 -The MSD recovery was outside acceptance limits, but passed duplicate spike acceptance criteria. The batch was accepted based on the accept~bility of the MS. CtF WO#: 22K0334 www.ChemtechFord.com mg/L SpkValue MRL DF 100 11 .0 1.00 Page 30 of 39 Analyte QC Sample ID: BWK0602-BLKl Date Prepared: 11/14/2022 Ammonia as N QC Sample ID: BWK0602-BSl Date Prepared: 11/14/2022 Ammonia as N QC Sample ID: BWK0602-MS1 Date Prepared: 11/14/2022 Ammonia as N QC Sample ID: BWK0602-MSD1 Date Prepared: 11/14/2022 Ammonia as N CtF WO#: 22K0334 www.ChemtechFord.com QC Report for Work Order (WO) -22K0334 % Rec RPO Limits RPO Max Result Source Cone Blank -EPA 350.1 Batch: BWK0602 Date Analyzed: 11/14/2022 Units: mg/L ND LCS -EPA 350.1 Batch: BWK0602 Date Analyzed: 11/14/2022 Units: mg/L 95.0 90 -110 0.950 Matrix Spike -EPA 350.1 Batch: BWK0602 QC Source Sample: 22K0334-0 I Date Analyzed: l l /14/2022 Units: mg/L 97.3 80 -120 1.01 0.0357 Matrix Spike Dup -EPA 350.1 Batch: BWK0602 QC Source Sample: 22K0334-0l Date Analyzed: 11/14/2022 Units: mg/L 102 4.29 80 -120 20 1.05 0.0357 SpkValue MRL OF 0.0500 1.00 1.00 0.0500 1.00 1.00 0.0500 1.00 1.00 0.0500 1.00 Page 31 of 39 QC Report for Work Order (WO) -22K0334 Analyte %Rec RPO Limits RPO Max Result Source Cone Blank -EPA 353.2 QC Sample ID: BWK0345-BLKJ Batch: BWK0345 Date Prepared: ll/08/2022 Date Analyzed: 1 J/08/2022 Units: Nitrate + Nitrite, Total, as N ND LCS -EPA 353.2 QC Sample ID: BWK0345-BS1 Batch: BWK0345 Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: Nitrate + Nitrite, Total, as N 93.0 80 -120 1.86 Matrix Spike -EPA 353.2 QC Sample ID: BWK0345-MS1 Batch: BWK0345 QC Source Sample: 22K0334-0l Date Prepared: 11 /08/2 022 Date Analyzed: 11 /08/2022 Units: Nitrate+ Nitrite, Total, as N 141 80 -120 1.41 ND QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO . QC Sample ID: BWK0345-MS2 Batch: BWK0345 QC Source Sample: XXXXXXX-XX Date Prepared: 11/08/2022 Date Analyzed: 11/08/2022 Units: Nitrate + Nitrite, Total, as N 97.0 80 -120 3.32 2.35 Matrix Spike Dup -EPA 353.2 QC Sample ID: BWK0345-MSD1 Batch: BWK0345 QC Source Sample: 22K0334-0 l Date Prepared: 11/08/2022 Date Analyzed: 11 /08/2022 Units: Nitrate + Nitrite, Total, as N 134 5.11 80 -120 20 1.34 ND QM-RPO -The recovery was outside acceptance limits for the MS and/or MSD. The RPO between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the acceptable recovery of the LCS and the RPO. QC Sample ID: BWK0345-MSD2 Date Prepared: l l /08/2022 Nitrate + Nitrite, Total, as N CtF WO#: 22K0334 www.ChemtechFord.com Batch: BWK0345 QC Source Sample: XXXXXXX-XX Date Analyzed: 11/08/2022 Units: 93.3 1.12 80 -120 20 3.28 2.35 mg/L mg/L mg/L mg/L mg/L mg/L Spk Value MRL OF 0.100 1.00 2.00 0.100 1.00 1.00 1.00 10.00 1.00 0.100 1.00 1.00 1.00 10.00 1.00 0.100 1.00 Page 32 of 39 QC Report for Work Order (WO) -22K0334 Analyte % Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Blank -EPA 8260D /5030A QC Sample ID: BWK.0262-BLKl Batch: BWK0262 Date Prepared: 11/04/2022 Date Analyzed: 11/04/2022 Units: ug/L Acetone ND 20.0 1.00 Benzene ND 1.0 1.00 Carbon Tetrachloride ND 1.0 1.00 Chloroform ND 1.0 1.00 Chloromethane ND 1.0 1.00 Methyl Ethyl Ketone ND 20.0 1.00 Methylene Chloride ND 1.0 1.00 Naphthalene ND 1.0 1.00 Tetrahydrofuran ND 1.0 1.00 Toluene ND 1.0 1.00 Xylenes, total ND 1.0 1.00 LCS -EPA 8260D /5030A QC Sample ID: BWK.0262-BSl Batch: BWK0262 Date Prepared: 11/04/2022 Date Analyzed: I 1/04/2022 Units: ug/L Acetone 114 70 -130 114 100 10.0 1.00 Benzene 89.3 70 -130 8.93 10.0 1.0 1.00 Carbon Tetrachloride 82.9 70 -130 8.29 10.0 1.0 1.00 Chloroform 95.7 70 -130 9.57 10.0 1.0 1.00 Chloromethane 122 70 -130 12.2 10.0 1.0 1.00 Methyl Ethyl Ketone 94.8 70 -130 94.8 100 10.0 1.00 Methylene Chloride 93.7 70 -130 9.37 10.0 1.0 1.00 Naphthalene 89.3 70 -130 8.93 10.0 1.0 1.00 Tetrahydrofuran 120 70 -130 12.0 10.0 1.0 1.00 Toluene 89.5 70 -130 8,95 10.0 1.0 1.00 Xylenes, total 88.9 70 -130 26.7 30.0 1.0 1.00 Matrix Spike -EPA 8260D /5030A QC Sample ID: BWK0262-MSI Batch: BWK0262 QC Source Sample: 22K0334-01 Date Prepared: 11/04/2022 Date Analyzed: 11/04/2022 Units: ug/L Acetone 110 70 -130 548 ND 500 50.0 1.00 Benzene 95.5 70 -130 47.8 ND 50.0 5.0 1.00 Carbon Tetrachloride 89.5 70 -130 44.8 ND 50.0 5.0 1.00 Chloroform 100 70 -130 50.2 ND 50.0 5.0 1.00 Chloromethane 130 70 -130 65.2 ND 50.0 5.0 1.00 Methyl Ethyl Ketone 93.4 70 -130 467 ND 500 50.0 1.00 Methylene Chloride 96.9 70 -130 48.4 ND 50.0 5.0 1.00 Naphthalene 89.4 70 -130 44.7 ND 50.0 5.0 1.00 Tetrahydrofuran 117 70 -130 58.4 ND 50.0 5.0 1.00 Toluene 96.2 70 -130 48.1 ND 50.0 5.0 1.00 Xylenes, total 96.0 70 -130 144 ND 150 5.0 1.00 Matrix Spike Dup -EPA 8260D /5030A QC Sample ID: BWK.0262-MSDl Batch: BWK.0262 QC Source Sample: 22K0334-0l Date Prepared: 11/04/2022 Date Analyzed: 11/04/2022 Units: ug/L Acetone 118 7.61 70 -130 20 591 ND 500 50.0 1.00 Benzene 96.6 1.15 70 -130 20 48.3 ND 50.0 5.0 1.00 Carbon Tetrachloride 90.0 0.557 70 -130 20 45.0 ND 50.0 5.0 1.00 Chloroform 102 1.97 70 -130 20 51 .2 ND 50.0 5.0 1.00 Ch loromethane 138 5.74 70 -130 20 69.0 ND 50.0 5.0 1.00 MS-High -Estimated high due to Matrix Spike recovery. Methyl Ethyl Ketone 101 7.34 70 -130 20 503 ND 500 50.0 1.00 CtF WO#: 22K0334 www. Chem tech Ford. com Page 33 of 39 Analyte QC Sample ID: BWK.0262-MSDI Date Prepared: 11/04/2022 Methylene Chloride Naphthalene Tetrahydrofuran Toluene Xylenes, total CtF WO#: 22K0334 www.ChemtechFord.com QC Report for Work Order (WO) -22K0334 %Rec RPO Limits RPO Max Result Source Cone Matrix Spike Dup -EPA 8260D /5030A (cont.) Batch: BWK.0262 QC Source Sample: 22K0334-01 Date Analyzed: 11/04/2022 Units: ug/L 103 5.81 70 -130 20 51 .4 ND 96.0 7.12 70 -130 20 48.0 ND 125 6.78 70 -130 20 62.5 ND 98.5 2.36 70 -130 20 49.2 ND 97.0 1.11 70-130 20 146 ND SpkValue MRL OF 50.0 5.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 150 5.0 1.00 Page 34 of 39 Analyte QC Sample ID: BWK0163-BLKI Date Prepared: 11 /03/2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) QC Sample ID: BWK0164-BLK1 Date Prepared: 11/03/2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) QC Sample ID: BWK0163-DUP1 Date Prepared: 11 /03/2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Alkalinity -Total (as CaCO3) QC Sample ID: BWK0164-DUP1 Date Prepared: 11/03/2022 Alkalinity -Bicarbonate (as CaCO3) Alkalinity -Carbonate (as CaCO3) Alkalinity -Total (as CaCO3) QC Sample ID: BWK0163-BSI Date Prepared: 11/03/2022 Alkalinity -Total (as CaCO3) QC Sample ID: BWK0164-BS1 Date Prepared: 11/03/2022 Alkalinity -Total (as CaCO3) CtF WO#: 22K0334 www.ChemtechFord.com QC Report for Work Order (WO) -22K0334 %Rec RPD Limits RPDMax Result Source Cone Spk Value MRL DF Blank -SM 2320 B Batch: BWK0163 Date Analyzed: I I /03/2022 Units: mg/L ND 1.0 1.00 ND 1.0 1.00 Batch: BWK0164 Date Analyzed: 11/03/2022 Units: mg/L ND 1.0 1.00 ND 1.0 1.00 Duplicate -SM 2320 B Batch: BWK0163 QC Source Sample: XXXXXXX-XX Date Analyzed: 11/03/2022 Units: mg/L 0.0964 20 104 104 1.0 1.00 20 ND ND 1.0 1.00 0.0964 20 104 104 1.0 1.00 Batch: BWK0164 QC Source Sample: 22K0334-01 Date Analyzed: 11/03/2022 Units: mg/L 1.63 20 310 305 1.0 1.00 20 ND ND 1.0 1.00 1.63 20 310 305 1.0 1.00 LCS -SM 2320 B Batch: BWK0163 Date Analyzed: 11 /03/2022 Units: mg/L 93.3 90 -110 220 236 1.0 1.00 Batch: BWK0164 Date Analyzed: 11/03/2022 Units: mg/L 94.9 90 -110 224 236 1.0 1.00 Page 35 of 39 Analyte QC Sample ID: BWK0243-BLK1 Date Prepared: 11/04/2022 Total Dissolved Solids (TDS) QC Sample ID: BWK0243-DUP1 Date Prepared: 11/04/2022 Total Dissolved Solids (TDS) QC Sample ID: BWK0243-DUP2 Date Prepared: I 1/04/2022 Total Dissolved Solids (TDS) QC Sample ID: BWK0243-BS1 Date Prepared: 11/04/2022 Total Dissolved Solids (TDS) CtF WO#: 22K0334 www.ChemtechFord.com QC Report for Work Order (WO) -22K0334 % Rec RPO Limits RPO Max Result Source Cone Blank -SM 2540 C Batch: BWK0243 Date Analyzed: 11 /04/2022 Units: mg/L ND Duplicate -SM 2540 C Batch: BWK0243 QC Source Sample: 22K0334-0l Date Analyzed: 11/04/2022 Units: mg/L 0.4 10 3930 3940 Batch: BWK0243 QC Source Sample: XXXXXXX-XX Date Analyzed: 11/04/2022 Units: mg/L 0.5 10 824 820 LCS -SM 2540 C Batch: BWK0243 Date Analyzed: 11/04/2022 Units: mg/L 105 90 -110 420 Spk Value MRL OF 10 1.00 20 1.00 20 1.00 400 20 1.00 Page 36 of 39 Surrogates Report for Work Order (WO) -22K0334 QC ID Analyte BWK0262-BLK1 1,2-Dichloroethane-d4 BWK0262-BLK1 4-Bromofluorobenzene BWK0262-BLK1 Toluene-dB BWK0262-BS1 1,2-Dichloroethane-d4 BWK0262-BS1 4-Bromofluorobenzene BWK0262-8S1 Toluene-dB BWK0262-MS1 1,2-Dichloroethane-d4 BWK0262-MS1 4-Bromofluorobenzene BWK0262-MS1 Toluene-dB BWK0262-MSD1 1,2-Dichloroethane-d4 BWK0262-MSD1 4-Bromofluorobenzene BWK0262-MSD1 Toluene-dB CtF WO#: 22K0334 www.ChemtechFord.com % Rec LCL UCL Result Blank -EPA 8260D /5030A 104 64.2 126 10.4 94.1 71.4 125 9.41 100 63.2 129 10.0 LCS -EPA 8260D /5030A 106 64.2 126 10.6 97.1 71.4 125 9.71 102 63.2 129 10.2 Matrix Spike -EPA 8260D /5030A 101 64.2 126 50.6 94.6 71.4 125 47.3 100 63.2 129 50.0 Matrix Spike Dup -EPA 8260D /5030A 105 64.2 126 52.6 93.8 71.4 125 46.9 100 63.2 129 50.0 SpkValue Batch DF 10.0 BWK0262 1.00 10.0 BWK0262 1.00 10.0 BWK0262 1.00 10.0 BWK0262 1.00 10.0 BWK0262 1.00 10.0 BWK0262 1.00 50.0 BWK0262 1.00 50.0 BWK0262 1.00 50.0 BWK0262 1.00 50.0 BWK0262 1.00 50.0 BWK0262 1.00 50.0 BWK0262 1.00 Page 37 of 39 Surrogate Recoveries (Field Samples) LabNumber Analyte 8260 Low Level Volatiles 22K0334-01 4-Bromofluorobenzene 22K0334-01 Toluene-d8 22K0334-01 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22K0334-02 1,2-Dichloroethane-d4 22K0334-02 22K0334-02 4-Bromofluorobenzene Toluene-d8 8260 Low Level Volatiles 22K0334-03 1,2-Dichloroethane-d4 22K0334-03 22K0334-03 4-Bromofluorobenzene Toluene-d8 8260 Low Level Volatiles 22K0334-04 1,2-Dichloroethane-d4 22K0334-04 22K0334-04 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22K0334-05 Toluene-d8 22K0334-05 22K0334-05 1,2-Dichloroethane-d4 4-Bromofluorobenzene 8260 Low Level Volatiles 22K0334-06 4-Bromofluorobenzene 22K0334-06 22K0334-06 Toluene-d8 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22K0334-07 1,2-Dichloroethane-d4 22K0334-07 22K0334-07 4-Bromofluorobenzene Toluene-d8 8260 Low Level Volatiles 22K0334-08 1,2-Dichloroethane-d4 22K0334-08 4-Bromofluorobenzene CtF WO#: 22K0334 www.ChemtechFord.com Result 9.63 10.0 10.1 10.4 9.73 10.0 10.1 9.56 10.1 10.3 9.42 10.2 10.2 10.5 9.20 9.39 10.0 10.3 10.4 9.74 10.0 10.6 9.39 Spklvl 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 %Rec 96.3 100 101 104 97.3 100 101 95.6 101 103 94.2 102 102 105 92.0 93.9 100 103 104 97.4 100 106 93.9 LCL UCL Qualifier 71.4 125 63.2 129 64.2 126 64.2 126 71.4 125 63.2 129 64.2 126 71.4 125 63.2 129 64.2 126 71.4 125 63.2 129 63.2 129 64.2 126 71.4 125 71.4 125 63.2 129 64.2 126 64.2 126 71.4 125 63.2 129 64.2 126 71.4 125 Page 38 of 39 22K0334-0B Toluene-dB 8260 Low Level Volatiles 22K0334-09 1,2-Dichloroethane-d4 22K0334-09 22K0334-09 4-Bromofluorobenzene Toluene-dB 8260 Low Level Volatiles 22K0334-10 Toluene-dB 22K0334-10 22K0334-10 1,2-Dichloroethane-d4 4-Bromofluorobenzene CtF WO#: 22K0334 www.ChemtechFord.com 10.0 10.6 9.46 10.0 10.0 10.2 9.77 10.0 10.0 10.0 10.0 10.0 10.0 10.0 100 106 94.6 100 100 102 97.7 63.2 129 64.2 126 71.4 125 63.2 129 63.2 129 64.2 126 71.4 125 Page 39 of 39 [ijijl Laboratories LLC a member of The GEL Group INC PO Box30712 Charleston.SC29417 2040 Savage Road Charleston. SC 29407 P 843.556.8171 F 843.766,1178 November 15, 2022 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: White Mesa Mill G W Work Order: 597226 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on October 18, 2022. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DW16138 Enclosures Sincerely, Julie Robinson Project Manager llll~U)III~ II 11111111111111111 II gel.com Page 2 of 29 SDG: 597226 Energy Fuels Resources (USA), Inc. White Mesa Mill GW SDG: 597226 November 15, 2022 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 597226 ample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on October 18, 2022 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following samples: Laboratory ID Client ID 597226001 MW-25 10102022 597226002 MW-11 10102022 597226003 MW-14 10112022 597226004 MW-31 10112022 597226006 MW-36 10112022 597226007 MW-05 10122022 597226008 MW-15 10122022 597226009 MW-28 10122022 597226010 MW-29 10122022 597226011 MW-12 10132022 597226012 MW-30 10132022 597226013 MW-26_10132022 597226014 MW-65_10132022 Case Narrative: Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. Page 3 of29 SDG: 597226 The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Page 4 of29 SDG: 597226 Julie Robinson Project Manager Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: _G_E_L_L_a_b_or_a_to_ri_es....:.,_L_L_C _______ Contact: Tanner Holliday 2040 Savage Road Ph: 435 678 2221 Charleston, SC 29407 tholliday@energyfuels.com (843) 556 8171 Chain of Custody/Sampling Analysis Request p . t roJec s amp ers N ame s amp ers s· t 1gna ure Q4 Ground Water 2022 Tanner Holliday l;)~P~ ~ ., Time Sample ID Date Collected Collected Laboratory Analysis Requested MW-25 10102022 10/10/2022 1040 Gross Alpha MW-11 10102022 10/10/2022 1400 Gross Alpha MW-14 10112022 10/11/2022 1450 Gross Alpha MW-31 10112022 10/11/2022 1310 Gross Alpha MW-32 10112022 10/11/2022 1145 Gross Alpha MW-36 10112022 10/11/2022 1435 Gross Alpha MW-05 10122022 10/12/2022 · 1415 Gross Alpha MW-15 10122022 10/12/2022 1030 Gross Alpha MW-28 10122022 10/12/2022 1350 Gross Alpha MW-29 10122022 10/12/2022 955 Gross Alpha MW-12 10132022 10/13/2022 905 Gross Alpha MW-30 10132022 10/13/2022 1010 Gross Alpha MW-26 10132022 10/13/2022 845 Gross Alpha MW-65 10132022 10/13/2022 905 Gross Alpha Comments: Please send report to Kathy Weinel at kweinel@energyfuels.com Relinquished BY,:(Sig~ature) ~~ft-...... ~ anner Holliday Page 5 of29 SDG: 597226 Date/Time Rteiv ma! I Laboratories : :/; Clienl: Received B : MVH Carrier and Tracking Number Suspected Hazard Information AlShi d as a DOT Hazardous? B) Did the diem designate the samples are to be received i'.L'i rndioaclivc'! C) Did the RSO cla.s.ify the samples as radioactive? ·oJ Die.I the dienr c.lesi nate sam les are hazardous? El Did the RSO identi ossihle hazanls? Sample Recei pl Criteria Shipping containers received intact and scaled? 2 'Chain of custody documents included with shipment'! 3 Samples requiring cold preservation within (0 < 6 de . C)?'' 4 D"ily check performed and passed on IR temperature gun? 5 Sample containers intact and sealed? 6 Samples requiring chemical preservation at proper pH? 7 Do any samples require Volatile Analysis? 8 Samples received within holding lime? 9 Sample ID's on COC match ID's on boules? Number of containers received match 11 number i 11dicated on COC? 12 Are sample containers identifiable as GEL rovided b use of GEL labels? 13 COC Form is properly signed in relinquished/received sections? Page 6 of29 SDG: 597226 Dale Received: FedEx Express Courier Other ~ ~ *lf Net Counls > lOOcpm on samples not m~ed "rmJimu.:live", conlact the Radiation Safety Gmup fur Lurthcr investi,galion. azard Class Shipped: UN#: If UN2910, Is the Radioactive Shipment Survey Complianl"? Yes_ No_ CDC notation or radioactive stickers on containeDi equal client designation. Maximum Net Counts Observed* (Observed Counts -Area Background Counts): CPM/mR/Hr Classilied as: Rad I Rad 2 Rad 3 / COC notation or hazard labels on containers equal client designation. f Dor Eis yes. select Hazards below. PCB's Flammable Foreign Soil RCRA Asbestos Beryllium Other. Commcnts/Qualiliers (Required for Non-Conforming Items) Circle Applicable: Seal-. broken Dmnugc:t.l con1ainer Leaking conrnincr 01her (describe) Circle Applicable: Clicnl cont:ic1cd and provided COC Presl!rvatiun Method: Wet ke kt! Packs Dry ice "'all lcmperarures arc recurtled in Celsius Temperature Device Serial #:~1R~2~-~21~---- Secondary Temperature Device Serial# (If Applicable): COC crcnl~d upon receipt Other. Circle Applicahlc: Seals broken Damaged container Leaking container 01hcr (dc.scrihcl le lD'.s and Conlilincrs Affcclcd: If Yes, are Encores or Soil Kits present for solids? Yes_ No_ NA_(lr yes. Lake 10 VOA Freezer) D liquid VOA vials contain acid preservation? Yes_ No_ NA_(lfunknown, select No) Are liquid VOA vials free ofheaclspace? Yes_ No_ NA_ !D's and tests affected: I D's and cuntuiner.i affected: Ci1Cle Applicable: No dales on containers No Limes on containers COC missing info Other (describe) Circle Applicable: No container count on COC Other (describe) Circle Applicable: Not relinquished Other (descrihe) GL-CHL-SR-001 Rev 7 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 597226 Q4 Ground Water 2022 ClientSDG: 597226 Project Manager: Julie Robinson Project Name: Purchase Order: DNMI00100 White Mesa Mill GW DW16138 Package Level: LEVEL3 EDD Format: EIM_DNMI GELID Client Sample ID Client Sample Desc. 597226001 MW-25_ 10102022 597226002 MW-11_ 10102022 597226003 MW-14_10112022 597226004 MW-31_10112022 597226006 MW-36_ 10112022 597226007 MW-05_ 10122022 597226008 MW-15_ 10122022 597226009 MW-28_ 10122022 597226010 MW-29 _ 10122022 597226011 MW-12_ 10132022 597226012 MW-30_ 10132022 597226013 MW-26_ 10132022 597226014 MW-65_ 10132022 Client Sample ID Status Tests/Methods -001 MW-25_10102022 REVW GFPC, Total Alpha Radium, Liquid -002 MW-11_10102022 REVW GFPC, Total Alpha Radium, Liquid -003 MW-14_ 10112022 REVW GFPC, Total Alpha Radium, Liquid -004 MW-31_10112022 REVW GFPC, Total Alpha Radium, Liquid -006 MW-36_10112022 REVW GFPC, Total Alpha Radium, Liquid -007 MW-05_10122022 REVW GFPC, Total Alpha Radium, Liquid -008 MW-15_10122022 REVW GFPC, Total Alpha Radium, Liquid -009 MW-28_10122022 REVW GFPC, Total Alpha Radium, Liquid -010 MW-29_10122022 REVW GFPC, Total Alpha Radium, Liquid -011 MW-12_10132022 REVW GFPC, Total Alpha Radium, Liquid -012 MW-30_10132022 REVW GFPC, Total Alpha Radium, Liquid Collect Date & Time 10-0CT -22 10:40 10-OCT-22 14:00 11-OCT -22 14:50 11-OCT-2213:10 11-OCT-2214:35 12-OCT-22 14:15 12-OCT-22 10:30 12-OCT -22 13:50 12-OCT-22 09:55 13-OCT-22 09:05 13-OCT-2210:10 13-OCT-22 08:45 13-OCT-22 09:05 Product Reference Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Work Order Due Date: 15-NOV-22 Package Due Date: EDD Due Date: Due Date: HM1 Receive Time # of Date & Time Zone Cont. 18-OCT -22 10:00 -2 1 18-OCT-22 10:00 -2 1 18-OCT-22 10:00 -2 , 18-OCT-22 10:00 -2 1 18-OCT-22 10:00 -2 1 18-OCT-22 10:00 -2 1 18-OCT-22 10:00 -2 1 18-OCT-22 10:00 -2 1 18-0CT-22 1 0:00 -2 1 18-OCT -22 1 0: 00 -2 1 18-OCT-22 10:00 -2 1 18-OCT-22 10:00 -2 1 18-OCT-22 10:00 -2 1 Fax Date PM Comments 15-NOV-22 15-NOV-22 15-NOV-22 Lab Matrix GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER Report Date: 15-NOV-22 Work Order: 597226 Page 1 of 2 Collector: C Prelogin #: 202210159602 Project Workdef ID: 1294356 SDG Status: Closed Logged by: Fax Days to Prelog Lab Field Due Date Process CofC# 20 20 20 20 20 20 20 20 20 20 20 20 20 Aux Data Group QC QC Receive Codes \0 N N r---°' l.f") ci Q if). °' N '+-< 0 r--- (!) ~ 0... GEL Laboratories LLC -Login Review Report -013 MW-26_10132022 -014 MW-65_10132022 REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid Product: GFCTORAL Workdef ID: 1458614 Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Gross Alpha Gross Alpha In Product Group? No Samples: 001, 002, 003, 004, 006, 007, 008, 009, 010, 011, 012, 013, 014 Parmname Check: All parmnames scheduled properly CAS# Contingent Tests Parmname Gross Radium Alpha Action Product Name Login Requirements: Requirement Description Group Name: Group Reference: Report Date: 15-NOV-22 Work Order: 597226 Page 2 of 2 Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Client RDL or PQL & Unit Reporting Parm Included Included Custom Units Function in Sample? in QC? List? pCi/L REG y y No Samples Include? Comments Peer Review by: ___________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? _____ _ \0 N ('I c--0\ V') ci o °' N ._ 0 00 ~ c<:S i:i... Heather Millar From: Sent: To: Kathy Weinel <KWeinel@energyfuels.com> Tuesday, October 18, 2022 1:03 PM Heather Millar Cc: N. Tanner Holliday; Team Robinson Subject: RE: GEL WO: 597226 Sample Preservation Heather, Please discard the sample. We will resample that well and send a new sample. K Energy Fuels Resources (USA Inc. Kathy Weinel Director, Regulatory Compliance t:303.389.4134I c: I f:303.389.4125 KWeinel@energyfuels.com 225 Union Blvd., Suite 600 Lakewood, CO 80228 http://www.energyfuels.com This e-mail is intended for the exclusive use of person(s) mentioned as the recipient(s). This message and any attached files with it are confidential and may contain privileged or proprietary information. If you are not the intended recipient(s) please delete this message and notify the sender. You may not use, distribute print or copy this message if you are not the intended recipient(s). From: Heather Millar <Heather.Millar@gel.com> Sent: Tuesday, October 18, 2022 10:33 AM To: Kathy Weinel <KWeinel@energyfuels.com> Cc: N. Tanner Holliday <tholliday@energyfuels.com>; Team Robinson <Team.Robinson@gel.com> Subject: GEL WO: 597226 Sample Preservation Good afternoon GEL received sample ID MW-32_10102022 this morning, October 18, 2022. Unfortunately, the sample did not hold any preservative. Would you like us to try to add more preservative? Please advise. Thank you, Heather Millar Project Manager Assistant Page 9 of 29 SDG: 597226 1 Laboratories LLC 4P 2040 Savage Road, Charleston, SC 29407 I P.O. Box 30712, Charleston, SC 29417 Office Main: 843.556.8171 I Office Fax: 843.769.7383 E-Mail: heather.millar@gel.com I Website: www.gel.com Follow us on Linkedln CONFIDENTIALITY NOTICE: This e-mail and any files transmitted with it are the property of The GEL Group, Inc. and its affiliates. All rights, including without limitation copyright, are reserved. The proprietary information contained in this e- mail message, and any files transmitted with it, is intended for the use of the recipient{s) named above. If the reader of this e-mail is not the intended recipient, you are hereby notified that you have received this e-mail in error and that any review, distribution or copying of this e-mail or any files transmitted with it is strictly prohibited. If you have received this e-mail in error, please notify the sender immediately and delete the original message and any files transmitted. 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To find out more, visit our website. 2 Page 10 of 29 SDG: 597226 List of current GEL Certifications as of 15 November 2022 State Certification Alabama 42200 Alaska 17-018 Alaska Drinking Water SC00012 Arkansas 88-0651 CLJA 42D0904046 California 2940 Colorado SC00012 Connecticut PH-0169 DoD ELAP/ ISO 17025 A2LA 2567.01 Florida NELAP £87156 Foreign Soils Permit P330-15-00283,P330-15-00253 Georgia SC00012 Georgia SDWA 967 Hawaii SC000I2 Idaho SC000I2 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SDWA 90129 Kentucky Wastewater 90129 Louisiana Drinking Water LA024 Louisiana NELAP 03046 (AI33904) Maine 2019020 Maryland 270 Massachusetts M-SC012 Massachusetts PF AS Approv Letter Michigan 9976 Mississippi SC000I2 Nebraska NE-OS-26-13 Nevada SC000 122023-3 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC000l2 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 2022-160 Pennsylvania NELAP 68-00485 Puerto Rico SC00012 S. Carolina Radiochem 10120002 Sanitation Districts of L 9255651 South Carolina Chemistry 10120001 Tennessee TN 02934 TexasNELAP Tl04704235-22-20 UtahNELAP SC000J22022-37 Vermont VT87156 Virginia NELAP 460202 Washington C780 Page 11 of 29 SDG: 597226 Radiochemistry Technical Case Narrative Energy Fuels Resources SDG #: 597226 Product: GFPC, Total Alpha Radium, Liquid Analytical Method: EPA 903.0 Analvtical Procedure: GL-RAD-A-044 REV# 10 Analytical Batch: 2336187 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 597226001 597226002 597226003 597226004 597226006 597226007 597226008 597226009 597226010 597226011 597226012 597226013 597226014 1205232196 1205232197 1205232198 1205232199 1205232200 lient am le Identification MW-25 10102022 MW-11 10102022 MW-14 10112022 MW-31 10112022 MW-36 10112022 MW-05 10122022 MW-15_10122022 MW-28 10122022 MW-29 10122022 MW-12 10132022 MW-30 10132022 MW-26 10132022 MW-65 10132022 Method Blank (MB) 59722600l(MW-25_10102022) Sample Duplicate (DUP) 59722600l(MW-25_10102022) Matrix Spike (MS) 597226001(MW-25_10102022) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Miscellaneous Information Additional Comments The matrix spike and matrix spike duplicate, 1205232198 (MW-25_10102022MS) and 1205232199 (MW-25_10102022MSD), aliquots were reduced to conserve sample volume. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the Page 12 of29 SDG: 597226 requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 13 of 29 SDG: 597226 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMIO0I Energy Fuels Resources (USA), Inc. Client SDG: 597226 GEL Work Order: 597226 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. ReviewNalidation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: j~ ~ Name: Theresa Austin Date: 15 NOV 2022 Title: Group Leader Page 14 of29 SDG: 597226 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Contact: Ms. Kathy Weinel Workorder: 597226 Parmname NOM Saf!!.ple Qual Rad Gas Flow 3atch 2336187 QC1205232197 597226001 DUP Gross Radium Alpha u 0.0554 u Uncertainty +l-0.189 QCl205232200 LCS Gross Radium Alpha 533 Uncertainty QC1205232 l 96 MB Gross Radium Alpha u Uncertainty QC 1205232 I 98 597226001 MS Gross Radium Alpha 2180 u 0.0554 Uncertainty +l-0.189 QC1205232199 597226001 MSD Gross Radium Alpha 2110 u 0.0554 Uncertainty +l-0.189 Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product QC Units 0.411 pCi/L +l-0.235 642 pCilL +l-6.59 -0.0665 pCilL +l-0.114 2060 pCilL +l-21.8 2060 pCilL +l-20.9 RPO% NIA 0.075 A B BD C D F H K L M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GCIMS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Page 28 of 29 SDG: 597226 Reoort Date: November 15, 2022 REC% Range Anlst NIA LXB3 121 (75%-125%) 94.4 (75%-125%) 97.4 (0%-20%) Page I of Date Time 11/14122 11 :2, 11/14122 11 :2 11/14122 11 :2, 1111412211:2 11/14122 11 :2 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 597226 Parmname -----NOM __§tmple Qual QC Units RPO% M Matrix Related Failure NIA RPD or %Recovery limits do not apply. See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification REC% Rang,1,__Anlst NI ND NJ Q R u UI UJ UL X y Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier h QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of Date Time NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. /\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where the duplicate value is less than 5X the RL, a control limit of +I-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 29 of 29 SDG: 597226 teJ ij • I Laboratories LLC a member of The GEL Group INC PO Box 30712 Chart eston. SC 29417 2040 Smge Road Charteston. SC 29407 P 843.556,8171 F 843.766.1178 November 22, 2022 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: White Mesa Mill G W Work Order: 598057 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on October 25, 2022. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO I 7025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DW16138 Enclosures Sincerely, ~1~ Julie Robinson Project Manager lll~HI IIII II 11 11111111111111111 gel.com Page 2 of 25 SDG: 598057 Energy Fuels Resources (USA), Inc. White Mesa Mill GW SDG: 598057 Novem her 22, 2022 Laboratorv Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 598057 ample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on October 25, 2022 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Id entification: The laboratory received the following samples: Laboratory ID Client ID 598057001 MW-17 10172022 598057002 MW-19_10172022 598057003 MW-18 10182022 598057004 MW-40_10182022 598057005 MW-01 10192022 598057006 MW-03A 10192022 598057007 MW-22 10192022 598057008 MW-27_10192022 598057009 MW-02 10202022 598057010 MW-39 10202022 Case Narrative: Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. Page 3 of 25 SDG: 598057 The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Page 4 of25 SDG: 598057 ~.1iiwc Julie Robinson Project Manager Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: GEL Laboratories, LLC Contact: Tanner Holliday -2-04_0_S_a_v_a_g_e __ R_o-ad_________ Ph : 435 678 222 1 Charleston, SC 29407 tholliday@energyfuels.com (843) 556 8171 Chain of Custody/Sampling Analysis Request Project Samplers Name Samplers Signature 04 Ground Water 2022 Tanner Holliday l~nAM~ _/,Lui~ , Time Sample ID Date Collected Collected Laboratory Analysis Requested MW-17 10172022 10/17/2022 1100 Gross Alpha MW-19 10172022 10/17/2022 1425 Gross Alpha MW-18 10182022 10/18/2022 1245 Gross Alpha MW-40 10182022 10/18/2022 1120 Gross Alpha MW-01 10192022 10/19/2022 1010 Gross Alpha MW-03A 10192022 10/19/2022 800 Gross Alpha MW-22 10192022 10/19/2022 1320 Gross Alpha MW-27 10192022 10/19/2022 1430 Gross Alpha MW-02 10202022 10/20/2022 910 Gross Alpha MW-39 10202022 10/20/2022 1030 Gross Alpha Comments: Please send report to Kathy Weinel at kweinel(@.energyfuels.com Relinquishe~~re) Datemme Received By:(Signature) Darmme 10/20/2022 M I u "1"(/, 'I... _j~ · Tanner Holliday 1100 ~ l I O{)l) Relinquished By: (Signature) Date/Time Reeeived By:"(Signature) Date/Time Page 5 of 25 SDG: 598057 m:a!J I Latloratones LLC Received B :MVH Carrier and Tracking Number Suspected Haz:ird Information A)Shi d as a DOT Hazanlous? B) Did the client designate the samples arc 10 he received a.~ radioacLivc'! C) Did the RSO classify the samples as radioacLive'? DJ Oit.l rhe client t.lesi are sam lcs are hazardous? El Did the RSO identi ssihle hazards? Swnple Receipt Criteria Shipping containers received intact and scaled? 2 Chain of custody documents included with shipment'? fV\»-1, I \t.Syz..-z.. 3 Samples requiring cold preservation within /0 :5. 6 de . Cl?* 4 Daily check performed anti passed on TR temperature gun? 5 Sample conlainers intact and sealed? 6 Samples requiring chemical preservation at proper pH? 7 Do any samples require Volatile Analysis? 8 Samples received within holding time? 9 Sample ID's on COC mulch TD's on bottles? 12 Are sample containers identifiable as GEL rovided bv use of GEL labels? 13 COC form is properly signed in relin uished/received sections? SAMPLE RECEIPT & REVIEW FORM K_ SDG/AR/COC/Work Date Received: \ FedEx Express Courier Other ~ ~ •If Net Counts> lOOcpm nn samples not marked "radioactive", conlacl the R.u.ljaliun Safety Gmup for further investigation. arnrd Class Shipped: UN#: Ir UN2910, Is the Rndioacti\'e Shipment Survey Compliant? Yes_ No_ aximum Net Counts Observed* (Observed Counts -Area Backgrnund Counts): -,,t:----r- Clossified ru;: Rad I Rad 2 Rad 3 COC notation or hazord label., on container.; equal client designation. / lf'D or Eis yes, select Hazards below. PCB's Flammable Foreign Soil RCRA Asbestos Beryllium Other: Commenls/Qualifiers (Required for Non-Conforming Items) Cin:lc Applicable: Seals broken Damag~d con1ainer Leaking con1uiner 01hcr (describe) Circle AppLic:iblc: Clicnl conl::ictcd and pro"idcd COC COC crcalcd upon rcccipl Preservation Method: Wet ke kt: Packs D,y ice Od1cr. *all temperatures are recorded in Celsius Temperature Device Serial #:.~IR~2~·~2~1 ____ _ Secondary Temperature Device Serial# (If Applicable): Damag.c:d container Leaking cnniaincr 01hcr (dcscrihcJ Do iquid VOA vials contain acid preservation? Yes_ No_ NA_(l[unknown, select No) re liquid VOA vials free ofheadspace? Yes_ No_ NA_ ID's and tests offcctcd: ID's and cantainen; .iffecte<l: Circle Applicable: No dates on containers No limes on containers COC missing info Other (describe) Ci <>-Applicable: No coer~ on COC Other (describe) Circle Arplicahlc: Not relinquished 0[her (describe) PM (or PMAJ review: Initials _________ Da[e _________ Page __ of GL-CHL-SR-001 Rev 7 Page 6 of25 SDG: 598057 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 598057 Client SDG: 598057 Project Manager: Project Name: Purchase Order: Package Level: EDD Format: Julie Robinson DNMI00100 White Mesa Mill GW DW16138 LEVEL3 EIM_DNMI GELID Client Sample ID Client Sample Desc. 598057001 MW-17_10172022 598057002 MW-19_10172022 598057003 MW-18_ 10182022 598057004 MW-40_ 10182022 598057005 MW-01_ 1 0192022 598057006 MW-03A_ 10192022 598057007 MW-22_ 10192022 598057008 MW-27 _ 10192022 598057009 MW-02_ 10202022 598057010 MW-39 _ 1 0202022 Client Sample ID Status Tests/Methods -001 MW-17_10172022 REVW GFPC, Total Alpha Radium, Liquid -002 MW-19_10172022 REVW GFPC, Total Alpha Radium, Liquid -003 MW-18_10182022 REVW GFPC, Total Alpha Radium, Liquid -004 MW-40_10182022 REVW GFPC, Total Alpha Radium, Liquid -005 MW-01_10192022 REVW GFPC, Total Alpha Radium, Liquid -006 MW-OJA_ 10192022 REVW GFPC, Total Alpha Radium, Liquid -007 MW-22_10192022 REVW GFPC, Total Alpha Radium, Liquid -008 MW-27_10192022 REVW GFPC, Total Alpha Radium, Liquid -009 MW-02_10202022 -010 MW-39_10202022 Collect Date & Time 17-OCT-2211:00 17-OCT-22 14:25 18-OCT -22 12:45 18-OCT-22 11 :20 1 9-OCT -22 1 O: 10 19-OCT -22 08:00 19-OCT -22 13:20 19-OCT-2214:30 20-OCT-22 09:10 20-OCT-22 10:30 Product Reference Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Work Order Due Date: 22-NOV-22 Package Due Date: EDD Due Date: Due Date: HM1 Receive Time # of Date & Time Zone Cont. 25-OCT-22 10:00 -2 1 25-OCT-22 10:00 -2 1 25-OCT-22 10:00 -2 1 25-OCT -22 10:00 -2 1 25-OCT -22 10:00 -2 1 25-OCT -22 10:00 -2 1 25-OCT -22 10:00 -2 1 25-OCT-22 10:00 -2 1 25-OCT-22 10:00 -2 1 25-OCT-22 10:00 -2 1 Fax Date PM Comments 22-NOV-22 22-NOV-22 22-NOV-22 Lab Matrix GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER Report Date: 22-NOV-22 Work Order: 598057 Page 1 of 2 Collector: C Prelogin #: 202210160026 Project Workdef ID: 1294356 SDG Status: Closed Logged by: Fax Days to Prelog Lab Field Due Date Process CofC# 20 20 20 20 20 20 20 20 20 20 Aux Data Group QC QC Receive Codes r--- lf) 0 00 0\ If) ci Cl r:/). If) N 4-< 0 r--- Q) ~ P-< GEL Laboratories LLC -Login Review Report Product: GFCTORAL Workdef ID: 1458614 Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Samples: 001, 002, 003, 004, 005, 006, 007, 008 Parmname Check: All parmnames scheduled properly CAS# Parmname Gross Radium Alpha In Product Group? No Action Product Name Description Contingent Tests Login Requirements: Requirement Group Name: Group Reference: Report Date: 22-NOV-22 Work Order: 598057 Page 2 of 2 Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Client RDL or PQL & Unit Reporting Parm Included Included Custom Units Function in Sample? in QC? List? pCi/L REG y y No Samples Include? Comments Peer Review by: ____________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? _____ _ r--- lr) 0 00 0--, lr) ci Cl if] lr) N 4-; 0 00 (1) ~ p.. Jessica Ward From: Sent: To: Cc: Subject: Kathy, Heather Millar Tuesday, October 25, 2022 3:54 PM Kathy Weinel; N. Tanner Holliday Team Robinson RE: GEL WO: 598057 Preservation Issue I do apologize for the inconvenience this is causing. I will let management know so we can hopefully avoid this in the future. Please let me know if there is anything else I can do for you. Thank you, Heather Millar Project Manager Assistant Laboratories LLC 4P 2040 Savage Road, Charleston, SC 29407 I P.O. Box 30712, Charleston, SC 29417 Office Main: 843.556.8171 I Office Fax: 843.769.7383 E-Mail: heather.millar@gel.com I Website: www.gel.com Follow us on Linkedln From: Kathy Weinel <KWeinel@energyfuels.com> Sent: Tuesday, October 25, 2022 3:46 PM To: Heather Millar <Heather.Millar@gel.com>; N. Tanner Holliday <tholliday@energyfuels.com> Cc: Team Robinson <Team.Robinson@gel.com> Subject: RE: GEL WO: 598057 Preservation Issue [E~ERNAL EMAIL] E>Gl N01' ~LI.CK Onks _pr:attac~merifs unless you recqg/liz~ the senaer and Rnow tne c_ontent Is safe. Heather, Please discard those samples -we will resample. More importantly, we get the sample bottles from GEL. This is the third time this quarter that we are resampling as a result of an elevated pH in what are supposed to be pre-preserved bottles. We have not had these issues prior in these wells -which leads me to believe it is a preservation issue with the GEL supplied bottles rather than a buffering issue with the GW. Please advise management that the bottles may be inadequately preserved or the preservative is old and ineffective. Please note that Utah will not accept samples that are not preserved at the time of receipt. So we are forced to resample. Also -these wells are a 4-5 hour purge time each prior to sampling. So at this point with the previous wells and this group of wells we are at almost 2 full days of labor time to resample due to inadequate preservation of the sample bottles. 1 Page 9 of 25 SDG: 598057 Thanks K Energy Fuels Resources (USA) Inc. Kathy Weinel Director, Regulatory Compliance t:303.389.4134I c: I f:303.389.4125 KWeinel@energyfuels.com 225 Union Blvd., Suite 600 Lakewood, CO 80228 http://www.energyfuels.com This e-mail is intended for the exclusive use of person(s) mentioned as the recipient(s). This message and any attached files with it are confidential and may contain privileged or proprietary infonmation. If you are not the intended recipient(s) please delete this message and notify the sender. You may not use, distribute print or copy this message if you are not the intended recipient(s). From: Heather Millar <Heather.Millar@gel.com> Sent: Tuesday, October 25, 2022 1:12 PM To: Kathy Weinel <KWeinel@energyfuels.com>; N. Tanner Holliday <tholliday@energyfuels.com> Cc: Team Robinson <Team.Robinson@gel.com> Subject: GEL WO: 598057 Preservation Issue Good afternoon, GEL received samples this morning October 25, 2022. A couple of the samples that came preserved did not hold the preservation. Would you like us to try to preserve them again? The IDs for the samples that did not hold their preservation are MW-02_10202022 and MW-39_10202022. Please advise. Thank you, Heather Millar Project Manager Assistant GEL LaboratoriesLLc 4P 2040 Savage Road. Charleston, SC 29407 I P.O. Box 30712. Charleston, SC 29417 Office Main: 843.556.8171 I Office Fax: 843.769.7383 E-Mail: heather.millar@gel.com I Website: www.gel.com Follow us on Linkedln CONFIDENTIALITY NOTICE: This e-mail and any files transmitted with it are the property ofThe GEL Group, Inc. and its affiliates. All rights, including without limitation copyright, are reserved. The proprietary information contained in this e- mail message, and any files transmitted with it, is intended for the use of the recipient(s) named above. If the reader of this e-mail is not the intended recipient, you are hereby notified that you have received this e-mail in error and that any review, distribution or copying of this e-mail or any files transmitted with it is strictly prohibited. If you have received this e-mail in error, please notify the sender immediately and delete the original message and any files transmitted. The 2 Page 10 of 25 SDG: 598057 unauthorized use of this e-mail or any files transmitted with it is prohibited and disclaimed by The GEL Group, Inc. and its affiliates. Disclaimer The information contained in this communication from the sender is confidential. It is intended solely for use by the recipient and others authorized to receive it. If you are not the recipient, you are hereby notified that any disclosure, copying, distribution or taking action in relation of the contents of this information is strictly prohibited and may be unlawful. This email has been scanned for viruses and malware, and may have been automatically archived by Mimecast, a leader in email security and cyber resilience. Mimecast integrates email defenses with brand protection, security awareness training, web security, compliance and other essential capabilities. Mimecast helps protect large and small organizations from malicious activity, human error and technology failure; and to lead the movement toward building a more resilient world. To find out more, visit our website. 3 Page 11 of 25 SDG: 598057 List of current GEL Certifications as of 22 November 2022 State Certification Alabama 42200 Alaska 17-018 Alaska Drinking Water SC00012 Arkansas 88-0651 CLIA 4200904046 California 2940 Colorado SC00012 Connecticut PH-0169 DoD ELAP/ ISO 17025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-15-00283,P330-15-00253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SDWA 90129 Kentucky Wastewater 90129 Louisiana Drinking Water LA024 Louisiana NELAP 03046 (A133904) Maine 2019020 Maryland 270 Massachusetts M-SC012 Massachusetts PF AS Approv Letter Michigan 9976 Mississippi SC00012 Nebraska NE-OS-26-13 Nevada SC000 122023-3 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 2022-160 Pennsylvania NELAP 68-00485 Puerto Rico SC00012 S. Carolina Radiochem 10120002 Sanitation Districts of L 9255651 South Carolina Chemistry 10120001 Tennessee TN 02934 TexasNELAP T104704235-22-20 UtahNELAP scooo 122022-3 7 Vermont VT87!56 Virginia NELAP 460202 Washington C780 Page 12 of 25 SDG: 598057 Radiochemistry Technical Case Narrative Energy Fuels Resources SDG #: 598057 Product: GFPC, Total Alpha Radium, Liquid Analvtical Method: EPA 903.0 Analytical Procedure: GL-RAD-A-044 REV# IO Analytical Batch: 2339842 The following samples were analyzed using the above methods and analytical procedure(s). Client Sample Identification MW-17 10172022 MW-19 10172022 MW-18 10182022 MW-40 10182022 MW-01 10192022 MW-03A 10192022 MW-22 10192022 MW-27 10192022 Method Blank (MB) GEL Sample ID# 598057001 598057002 598057003 598057004 598057005 598057006 598057007 598057008 1205239748 1205239749 1205239750 1205239751 1205239752 59805700I(MW-17_10172022) Sample Duplicate (DUP) 598057001(MW-17_10172022) Matrix Spike (MS) 598057001 (MW-17 _IO 172022) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (QC) Information RDLMet The following RDL was met with rounding. Sample Analyte Value 1205239749 (MW-17_10172022DUP) Gross Radium Alpha Result 0.895 < MDA 1.12 > RDL 1 pCi/L Miscellaneous Information Additional Comments The matrix spike and matrix spike duplicate, 1205239750 (MW-17 _10172022MS) and 1205239751 (MW-17_10172022MSD), aliquots were reduced to conserve sample volume. Page 13 of 25 SDG: 598057 Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 14 of25 SDG: 598057 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMIO0I Energy Fuels Resources (USA), Inc. Client SDG: 598057 GEL Work Order: 598057 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. ReviewNalidation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: j~ ~ Name: Theresa Austin Date: 22 NOV 2022 Title: Group Leader Page 15 of 25 SDG: 598057 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summarr Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Contact: Ms. Kathy Weinel Workorder: 598057 Parmname ---NOM Sample _Qual Rad Gas Flow 3atch 2339842 QC1205239749 598057001 DUP Gross Radium Alpha u 0.201 u Uncertainty +l-0.236 QC1205239752 LCS Gross Radium Alpha 533 Uncertainty QC1205239748 MB Gross Radium Alpha u Uncertainty QC1205239750 598057001 MS Gross Radium Alpha 2110 u 0.201 Uncertainty +l-0.236 QC1205239751 598057001 MSD Gross Radium Alpha 2150 u 0.201 Uncertainty +l-0.236 Notes: Counting Uncertainty is calculated at the 68% confidence level ( I-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product QC Units 0.895 pCi/L +l-0.382 450 pCi/L +l-5.31 -0.191 pCilL +l-0. 148 1750 pCilL +l-21.4 1660 pCilL +/-20.1 RPO% NIA 5.36 A B BO C D F H K L M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Page 24 of 25 SDG: 598057 Reoort Date: November 22, 2022 REC% Rane Anlst NIA JXK3 84.4 (75%-125%) 82.9 (75%-125%) 77.4 (0%-20%) Page I of Date Time 11120122 14:2 11/20122 14:2 11120122 14:2 11/20122 14:2 11/20122 14:2 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 598057 Parmname NOM QC Units ~R_P~D_0_¼ __ R_E_C_% ___ R_an e Anlst M Matrix Related Failure NIA RPO or %Recovery limits do not apply. NI ND NJ Q R u UI UJ UL X y /\ h See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPO of sample and duplicate evaluated using +I-RL. Concentrations are <SX the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of Date Time NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPO not applicable. /\ The Relative Percent Difference (RPO) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (SX) the contract required detection limit (RL). In cases where the duplicate value is less than SX the RL, a control limit of +I-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SOIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 25 of 25 SDG: 598057 le;l 3 II Laboratories LLC a member of The GEL Group INC PO Box 30712 Chatleston. SC 29417 2040 Savage Road Chatleston. SC 29407 P 843.556.8171 F 843.766.1178 December 06, 2022 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: White Mesa Mill G W Work Order: 599611 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on November 04, 2022. This revised data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Package has been revised to reflect the correct sample ID and collection date for sample MW-70_10312022. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DW16138 Enclosures Sincerely Julie Robinson Project Manager llll ~IIIIIIIIII Ill 111111111111111 gel.co m Page 2 of 28 SDG: 599611 Revl Energy Fuels Resources (USA), Inc. White Mesa Mill GW SDG: 599611 Package has been revised to reflect the correct sample ID and collection date for sample MW-70 _ 10312022. December 06, 2022 Laboratorv [dentification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 599611 Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on November 04, 2022 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. ample Identification: The laboratory received the following samples: Laboratory ID Client ID 599611001 MW-35 10312022 599611002 MW-32 10312022 599611003 MW-02 11012022 599611004 MW-20_11012022 599611005 MW-23 11012022 599611006 MW-37 11012022 599611007 MW-38 I 1012022 599611008 MW-39 _11012022 599611009 MW-70 10312022 599611010 TW4-24 11012022 59961101 I MW-24 11022022 599611012 MW-24A_l 1022022 Case Narrative: Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. Page 3 of28 SDG: 599611 Revl The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Page 4 of 28 SDG: 599611 Revl Julie Robinson Project Manager t 7:N~RGYFUELS RESOURCES Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: _G_E_L_L_a_b_or_a_to_ri_es_,_L_L_C _______ Contact: Tanner Holliday 2040 Savage Road Ph: 435 678 2221 Charleston, SC 29407 tholliday@energyfuels.com (843) 556 8171 Chain of Custody/Sampling Analysis Re uest p . t ro1ec s ampers N ame s amp ers s· t 19na ure / Q4 Ground Water 2022 Tanner Holliday I \/AAlllrl~J/4//~/ -· , Time Sample ID Date Collected Collected Laboratory Analysis Requested MW-35 10312022 10/31/2022 1345 Gross Alpha MW-32 10312022 10/31/2022 1300 Gross Alpha MW-02 11012022 11/1/2022 955 Gross Aloha MW-20 11012022 11/1/2022 1200 Gross Alpha MW-23 11012022 11/1/2022 1245 Gross Aloha MW-37 11012022 11/1/2022 1305 Gross Alpha MW-38 11012022 11/1/2022 1230 Gross Aloha MW-39 11012022 11/1/2022 1120 Gross Alpha MW-70 11012022 11/1/2022 1345 Gross Alpha TW4-24 11012022 11/1/2022 1330 Gross Alpha MW-24 11022022 11/2/2022 645 Gross Alpha MW-24A 11022022 11/2/2022 700 Gross Alpha Comments: Please send report to Kathy W einel at kweinel@energyfuels.com Page 5 of 28 SDG: 599611 Revl Date/Time Received By:(Signature) 11/2/2022 1130 Date/Time Date/Time I I -(j ·22 1010 Datemme rnE I Laboratories LLC SAMPLE RECEIPT & REVIEW FORM Client: ()NM, SDG/AR/COC/Work Order. Br/6/1 Receh•ed n v: fvl.L~ Dnle Received: lo ·c..f ·1,,,-? FedEx Express Circ~bl,: FedEx Ground PS Field Services Courier Olher Carrier and Tracking Number 1-l t<l"=i l?'-lY o?.. Cf ~IC\ 9 7 ri+ Suspected Hn7.llrd Infonnotion ri 0 • If Ncl Counts> IO<kpm on s:unplc• not marked "r.ulioactivc", contact the R.1di11tion Snfoly Group for runltcrinvcsri~"'tion. :,.. z I H.a.anl Class Shipped: UN#: A)Shinned o.s a DOT Hnzanlous'/ tr UN29 I 0, Is tho Radioocrivc Shipment Survey Complirun7 Yes_ No_ B) Did the client designate the s:unplcs an, 10 be ( COC no1:11ion or ratlionctive stickers on c:o111ui11crs equal client designation. received as radioactive7 C) Did lhe RSO classify the sampl>!S a.< I M._,imum Net Counts Observed• (Observed Counts. Arcu Backi;round Counts): ~mll/llr I11dio~ct'""' Clnssilicd ns: Rael I nnd 2 Rnd 3 D) Did lhc client dcsh!11ote s:unnlcs :uc hazurdous·/ I COC no101ion ur hll:zard labds on cunlainers equal client de.i!l'lation. I If D or E i• yes, select fl:izortls below. E) Did the RSO idcntifv oossiblc hll7,irds? PCB's Flammable Poir.ign Soil RCRA Asbestos Bccyllium Od1cr: Snmplc Receipt Critcrin r; < C, Comrnents/Qunlificrs (Required fur Nun-Confonnlng Items) > z z Shipping containers received intact and i Circl" AppOcoblc: Scol< h<okcn Dlffl:at,-.:d conu,fni:r U!uldng cun111incr Oilier (dc<.:nno) l :.eal~d7 / ii 2 Chain of custody documents included I I Circle Applic:ihlo: Clkn, coo1:1ch!J .2nd provided COC COC crc-3tcJ uvon rccclpl with sl,ipment'/ rrucrvatiun Method: Wet la: [c,: Packs Dey icc~ther: TEMP:ZDC:-3 Samples requiring cold preservation I ""11 tcmpcrarurcs ore rccnn!ed in Cclsill< • wlthin (0 S 6 def. C)?• ..,. "'-- Doily check performed and pos.scd on JR / ffl Ten1perulur< Oc\'lco Serial #: ".J,,'1'L. 7~ 4 tcmpcr.uurc gun1 S«ondwyTcrupcmturc Deviu: Serini fl (If Applicahlc}: ,l /l C'1-c:1, ,\11pllc:,blu: Sc:11$ broken O;n1il~ctl coot:1int;1r Lc:i.ki11,;: conwiiac:r 01hcr (dc.<cnoo) 5 Snmplc contuincrs intuct und scaled'/ Samples requiring chemicul preservation I Smup1c: 10·1 w,tJ Con1:airacri Affi:tlcd: 6 at proper pH'/ If Pn.:.si:n-:a,iun nJJclJ, Lutrt: If Y os, nre Encores or Soll Kits prcsclll for solid$' Y 0$ No NA (If Y(S. loku to VOA Frcc~.a:r) Do nny samples require Volatile Do liquid. VOA vials contain ocld proservotinn? Yes No t,IA (If unknown, select l'fo) .. 7 Analysis? .\·/ Are liquid VOA viols fll!c: ofhc,dsp:11.-.:? Yes_ No_ NA_ :It: S::impJc ID's :mJ cont.aini:rs :1ffi:ctcd: ~ ID"s ond \cs~, affected: 8 Samples received within holding time? / ~ . Sample ID's on COC ffilltch !D's on i !D's and cnn1runcr., off«1cd: 9 bellies? r Date & time on COC match data&. lime Circle Applicable: No datci on contruocrs No 1in1c.,i;; nn cont.Uncrs COC missin& info Od1er (describe) 10 on bottles? ( N"umbcr of containers received mulch Circle Applicable: No comruncr cnun1 on CQC Other (describe) 11 number indicated on COC? / "· • 12 Ale lillmple c<.mlllincr:; itlcntifiublc as :m GEL orovidcd bv use of Gl!L labels? 13 COC form is properly signed in Circle Applkublc: Not n,linqui,hed Other (doscribc) rclinquisl1cll/rccclvcd sections? Commcnl$ (U5c Cun1in1rntion Fonn if needed): PM (or PMA) review: lnitfals ..)f/L Dntc {(-'"J-7 7 Pose __l_ of GL-CHL-SR-001 Rev7 . Page 6 of28 SDG: 599611 Revl GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 599611 Client SDG: 599611 Q4 Ground Water 2022 Project Manager: Project Name: Purchase Order: Package Level: EDD Format: Julie Robinson DNMI00100 White Mesa Mill GW DW16138 LEVEL3 EIM_DNMI GELID Client Sample ID Client Sample Desc. 599611001 MW-35 _ 10312022 599611002 MW-32_10312022 599611003 MW-02_11012022 599611004 MW-20_11012022 599611005 MW-23_ 11012022 599611006 MW-37 _ 11012022 599611007 MW-38_ 11012022 599611008 MW-39_ 11012022 599611009 MW-70_ 10312022 599611010 TW4-24_ 11012022 599611011 MW-24_ 11022022 599611012 MW-24A_ 11 022022 Client Sample ID Status Tests/Methods -001 MW-35_10312022 REVW GFPC, Total Alpha Radium, Liquid -002 MW-32_10312022 REVW GFPC, Total Alpha Radium, Liquid -003 MW-02_11012022 REVW GFPC, Total Alpha Radium, Liquid -004 MW-20_11012022 REVW GFPC, Total Alpha Radium, Liquid -005 MW-23_11012022 REVW GFPC, Total Alpha Radium, Liquid -006 MW-37_11012022 REVW GFPC, Total Alpha Radium, Liquid -007 MW-38_11012022 REVW GFPC, Total Alpha Radium, Liquid -008 MW-39_11012022 REVW GFPC, Total Alpha Radium, Liquid -009 MW-70_10312022 REVW GFPC, Total Alpha Radium, Liquid -010 TW4-24_11012022 REVW GFPC, Total Alpha Radium, Liquid -011 MW-24_11022022 REVW GFPC, Total Alpha Radium, Liquid -012 MW-24A_ 11022022 REVW GFPC, Total Alpha Radium, Liquid Collect Date & Time 31-OCT-22 13:45 31-OCT-2213:00 01-NOV-22 09:55 01-NOV-22 12:00 01-NOV-22 12:45 01-NOV-22 13:05 01-NOV-2212:30 01-NOV-22 11 :20 31-OCT-22 13:45 01-NOV-22 13:30 02-NOV-22 06:45 02-NOV-22 07:00 Product Reference Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Work Order Due Date: 05-DEC-22 Package Due Date: EDD Due Date: Due Date: AJ1 Receive Time # of Date & Time Zone Cont. 04-NOV-22 10:10 -2 1 04-NOV-22 10:10 -2 1 04-NOV-22 10:10 -2 1 04-NOV-22 10:10 -2 1 04-NOV-22 10:10 -2 1 04-NOV-22 10:10 -2 1 04-NOV-22 10:10 -2 1 04-NOV-22 10:10 -2 , 04-NOV-22 10:10 -2 1 04-NOV-2210:10 -2 1 04-NOV-2210:10 -2 1 04-NOV-22 10:10 -2 1 Fax Date PM Comments 05-DEC-22 05-DEC-22 05-DEC-22 Lab Matrix GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER GROUND WATER Report Date: 06-DEC-22 Work Order: 599611 Page 1 of 2 Collector: C Prelogin #: 202211160908 Project Workdef ID: 1294356 SDG Status: Closed Logged by: Fax Days to Prelog Lab Field Due Date Process CofC# Group QC QC 20 20 20 20 20 20 20 20 20 20 20 20 Receive Aux Data Codes ...... > (I) ~ ...... ...... \0 °" °" tr) ci Q r:/) 00 N 4-< 0 t"-- (I) OJ) ctj A-< GEL Laboratories LLC -Login Review Report Product: GFCTORAL Workdef ID: 1458614 In Product Group? No Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Samples: 001, 002, 003, 004, 005, 006, 007, 008, 009, 010, 011, 012 Parmname Check: All parmnames scheduled properly CAS# Contingent Tests Parmname Gross Radium Alpha Action Product Name Login Requirements: Requirement Description Group Name: Group Reference: Report Date: 06-DEC-22 Work Order: 599611 Page 2 of 2 Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Client RDL or PQL & Unit Reporting Parm Included Included Custom Units Function in Sample? in QC? List? pCi/L REG y y No Samples Include? Comments Peer Review by: ____________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? _____ _ ...... > ~ ...... ...... \0 °' °' lr) d Cl r/1 00 N 4-< 0 00 Q) ~ 0-. Julie Robinson From: Sent: To: Cc: Subject: Attachments: Julie, Kathy Weinel < KWeinel@energyfuels.com > Monday, December 5, 2022 11 :36 AM Julie Robinson N. Tanner Holliday; Jordan Christine App FW: Results for GEL SDG 599611 599611.pdf We had a small goof on the COC for the attached SDG. The sample collection date and Field Sample ID (EFRI Sample number) for MW-70 is incorrect on the COC. The correct sample date is actually 10/31/2022 and the EFRI number is MW-70_10312022. Unfortunately, I will need a corrected hardcopy package and a corrected Locus EDD. My apologies -these things happen! Let me know if you need a corrected COC and we will send t over ASAP. Thanks! Kathy Energy Fuels Resources (USA) Inc. Kathy Weinel Director, Regulatory Compliance t:303.389.4134 I c: I f:303.389.4125 KWeinel@energyfuels.com 225 Union Blvd., Suite 600 Lakewood, CO 80228 http://www.energyfuels.com This e-mail is intended for the exclusive use of person(s) mentioned as the recipient(s). This message and any attached files with it are confidential and may contain privileged or proprietary information. If you are not the intended recipient(s) please delete this message and notify the sender. You may not use, distribute print or copy this message if you are not the intended recipient(s). -----Original Message----- 1 Page 9 of28 SDG: 599611 Revl From: GEL Data <data@gellaboratories.com> Sent: Monday, December 5, 2022 7:10 AM To: Kathy Weinel <KWeinel@energyfuels.com>; N. Tanner Holliday <tholliday@energyfuels.com> Cc: vonda.fields@gel.com; Julie.Robinson@gel.com Subject: Results for GEL SDG 599611 Attached are the results for samples received at GEL Laboratories, LLC on November 04, 2022. Results have also been posted to the GEL website. Please notify your Project Manager is you have any questions. Thank you, Julie Robinson Do not reply to data@gellaboratories.com as this email address is not monitored. Please contact your project manager, Julie Robinson, at Team.Robinson@gel.com regarding this message or its attachments. Disclaimer The information contained in this communication from the sender is confidential. It is intended solely for use by the recipient and others authorized to receive it. If you are not the recipient, you are hereby notified that any disclosure, copying, distribution or taking action in relation of the contents of this information is strictly prohibited and may be unlawful. This email has been scanned for viruses and malware, and may have been automatically archived by Mimecast, a leader in email security and cyber resilience. Mimecast integrates email defenses with brand protection, security awareness training, web security, compliance and other essential capabilities. Mimecast helps protect large and small organizations from malicious activity, human error and technology failure; and to lead the movement toward building a more resilient world. To find out more, visit our website. 2 Page 10 of28 SDG: 599611 Revl List of current GEL Certifications as of06 December 2022 State Certification Alabama 42200 Alaska 17-018 Alaska Drinking Water SC00012 Arkansas 88-0651 CUA 42D0904046 California 2940 Colorado SC00012 Connecticut PH-0169 DoD ELAP/ ISOl7025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-15-00283,P330-15-00253 Georgia SC00012 Georgia SOWA 967 Hawaii SC00012 Idaho SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SDWA 90129 Kentucky Wastewater 90129 Louisiana Drinking Water LA024 Louisiana NELAP 03046 (AI33904) Maine 2019020 Maryland 270 Massachusetts M-SC012 Massachusetts PF AS Approv Letter Michigan 9976 Mississippi SC00012 Nebraska NE-OS-26-13 Nevada scooo 122023-3 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SOWA 45709 North Dakota R-158 Oklahoma 2022-160 Pennsylvania NELAP 68-00485 Puerto Rico SC00012 S. Carolina Radiochem 10120002 Sanitation Districts of L 9255651 South Carolina Chemistry 10120001 Tennessee TN 02934 TexasNELAP Tl04704235-22-20 Utah NELAP scooo 122022-3 7 Vermont VT87156 Virginia NELAP 460202 Washington C780 Page 11 of 28 SDG: 599611 Revl Radiochemistry Technical Case Narrative Energy Fuels Resources SDG #: 599611 Product: GFPC, Total Alpha Radium, Liquid Analvtical Method: EPA 903.0 Analytical Procedure: GL-RAD-A-044 REV# 10 Analytical Batch: 2339842 The following samples were analyzed using the above methods and analytical procedure(s). Client ample Identification MW-35 10312022 MW-32 10312022 MW-02 11012022 MW-20_11012022 MW-23 11012022 MW-37 11012022 MW-38_11012022 MW-39 11012022 MW-70 10312022 TW4-24 11012022 MW-24 11022022 MW-24A_l 1022022 Method Blank (MB) GEL Sample ID# 599611001 599611002 599611003 599611004 599611005 599611006 599611007 599611008 599611009 599611010 599611011 599611012 1205239748 1205239749 1205239750 1205239751 1205239752 59805700l(MW-17_10172022) Sample Duplicate (DUP) 59805700l(MW-17_10172022) Matrix Spike (MS) 598057001(MW-17_10172022) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (OC) Information RDLMet The following RDL was met with rounding. Sample Analyte Value 1205239749 (MW-17_10172022DUP) Gross Radium Alpha Result 0.895 < MDA 1.12 > RDL 1 pCi/L Miscellaneous Information Additional Comments The matrix spike and matrix spike duplicate, 1205239750 (MW-17 _10172022MS) and 1205239751 Page 12 of 28 SDG: 599611 Revl (MW-17 _IO l 72022MSD), aliquots were reduced to conserve sample volume. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 13 of28 SDG: 599611 Revl GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMIO0 1 Energy Fuels Resources (USA), Inc. Client SDG: 599611 GEL Work Order: 599611 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. Review/Validation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: j~ ~ Name: Theresa Austin Date: 06 DEC 2022 Title: Group Leader Page 14 of 28 SDG: 599611 Revl GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Contact: Ms. Kathy Weinel Workorder: 599611 Parmname NOM Samp~ ual Rad Gas Flow 3atch 2339842 QC1205239749 598057001 DUP Gross Radium Alpha u 0.201 u Uncertainty +l-0.236 QC1205239752 LCS Gross Radium Alpha 533 Uncertainty QC!205239748 MB Gross Radium Alpha u Uncertainty QC1205239750 598057001 MS Gross Radium Alpha 2110 u 0.201 Uncertainty +l-0.236 QC1205239751 598057001 MSD Gross Radium Alpha 2150 u 0.201 Uncertainty +l-0.236 Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product QC Units ---- 0.895 pCilL +l-0.382 450 pCilL +l-5.31 -0. 191 pCilL +l-0.148 1750 pCilL +l-21.4 1660 pCilL +l-20.1 RPD¾ NIA 5.36 A B BD C D F H K L M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Page 27 of 28 SDG: 599611 Revl Reoort Date: December 6, 2022 REC% Rane Anlst NIA JXK3 84.4 (75%-125%) 82.9 (75%-125%) 77.4 (0%-20%) Page 1 of Date Time 11120122 14:2 11120122 14:2 11120122 14:2 I 1120122 14:2 11120/22 14:2 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 599611 Page 2 of Parm name NOM Sam(lle ~ QL U_n•~·ts~_R-'---=-P=D~0/4 REC% Ran,.ge Anlst Date Time M Matrix Related Failure NIA RPD or %Recovery limits do not apply. NI ND NJ Q R u UI UJ UL X y /\ h See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. "The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where the duplicate value is less than 5X the RL, a control limit of +I-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 28 of28 SDG: 599611 Revl TabF Laboratory Analytical Reports -Accelerated Monitoring Tab Fl Laboratory Analytical Reports -Accelerated Monitoring November 2022 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-11_11082022 Matrix: Water Date Sampled: 11/8/22 12:30 Chloride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \ldals Manganese, Dissolved Result 71.9 2.74 1140 2270 0.220 Project Name: November Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 1.00 0.100 50.0 20 0.0100 PO#: Receipt: 11/11/22 10:45@ 0.3 °C Date Reported: 12/2/2022 Project Name: November Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 CtF WO#: 22K0963 Preparation Date/Time 11/15/22 I 1/21/22 I 1/11/22 11/11/22 I 1/21/22 Lab ID: 22K0963-01 Analysis Date/Time 11/16/22 I 1/21/22 I 1/14/22 I 1/11/22 I 1/21/22 .fulilll Page 3 of 18 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD Serving the lntermountain West Since 1953 LABORATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-25_11092022 Matrix: Water Date Sampled: 11/9/22 11:10 I nor~anic Total Dissolved Solids (TDS) 2690 Project Name: November Ground Water 2022 www.ChemtechFord.com Units mg/L Certificate of Analysis Minimum Reporting !J.mi! 20 PO#: Receipt: 11/11/22 10:45@ 0.3 °C Date Reported: 12/2/2022 Project Name: November Ground Water 2022 Sampled By: Tanner Holliday ~ SM2540C CtF WO#: 22K0963 Preparation Date/Time 11/14/22 Lab ID: 22K0963-02 Analysis Date/Time 11/14/22 .E!.ailll Page 4 of 18 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 lA80R,\TOA1£S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-26_11102022 Matrix: Water Date Sampled: 11/10/22 7:15 lnor~anic Chloride Nitrate+ Nitrite, Total, as N \'olalilc Or~anil' ( ·0111po11nd, Chloroform 59.2 0.408 512 Project Name: November Ground Water 2022 www.ChemtechFord.com mg/L mg/L ug/L Certificate of Analysis Minimum Reporting Limit 1.00 0.100 50.0 PO#: Receipt: 11/11/22 10:45@ 0.3 °C Date Reported: 12/2/2022 Project Name: November Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 EPA 8260D 15030A CtF WO#: 22K0963 Preparation Date/Time 11/15/22 I 1/21/22 11/16/22 Lab ID: 22K0963-03 Analysis Date/Time 11/16/22 I 1/21/22 I 1/16/22 ~ QM-4X Page 5 of 18 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/~BORATO RI ES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-30_11092022 Matrix: Water Date Sampled: 11/9/22 10:35 lnorl-(anic Chloride Nitrate+ Nitrite, Total, as N i\lctals Selenium, Dissolved Uranium, Dissolved Result 156 15.9 0.0756 0.0101 Project Name: November Ground Water 2022 www.ChemtechFord.com mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 5.00 0.500 0.0050 0.0003 PO#: Receipt: 11/11/22 10:45@ 0.3 °C Date Reported: 12/2/2022 Project Name: November Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 EPA200.8 EPA200.8 CtF WO#: 22K0963 Preparation Date/Time 11/16/22 11/21/22 11/21/22 11/21/22 Lab ID: 22K0963-04 Analysis Date/Time 11/17/22 11/21/22 11/21/22 11/21/22 .E!illrul Page 6 of 18 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD Serving the lntermountain West Since 1953 Ll~BORATOl!IEti Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-31_11082022 Matrix: Water Date Sampled: 11/8/22 14:20 lnor~anic Chloride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) Uranium, Dissolved Result 243 16.0 1380 2670 0.0245 Project Name: November Ground Water 2022 www. Chem tech Ford. com Units mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 5.00 0.500 20.0 20 0.0003 PO#: Receipt: 11/11/22 10:45@ 0.3 °C Date Reported: 12/2/2022 Project Name: November Ground Water 2022 Sampled By: Tanner Holliday ~ EPA300.0 EPA353.2 EPA300.0 SM2540 C EPA200.8 CtF WO#: 22K0963 Preparation Date/Time I 1/15/22 ll/21/22 ll/28/22 I 1/11/22 II/21/22 Lab ID: 22K0963-05 Analysis Date/Time 11/16/22 I 1/21/22 I 1/29/22 I 1/11/22 I 1/21/22 Page 7 of 18 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD Serving the lntermountain West Since 1953 L/~60RATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-65_11092022 Matrix: Water Date Sampled: 11/9/22 10:35 Inorganic Chloride Nitrate+ Nitrite, Total, as N i\lctals Selenium, Dissolved Uranium, Dissolved Result 183 15.7 0,0768 0.0104 Project Name: November Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 5.00 0.500 0.0050 0.0003 PO#: Receipt: 11/11/22 10:45@ 0.3 ·c Date Reported: 12/2/2022 Project Name: November Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 EPA200.8 EPA200.8 CtF WO#: 22K0963 Preparation Date/Time 11/15/22 11/21/22 11/21/22 11/21/22 Lab ID: 22K0963-06 Analysis Date/Time 11/16/22 11/21/22 11/21/22 11/21/22 Page 8 of 18 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com CHEMTECH·FORD Serving the lntermountain West Since 1953 Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 11/10/22 7:15 \'olatilc Organic Com rounds Chloroform Result < 1.0 Project Name: November Ground Water 2022 www. Chem tech Ford. com Units ug/L Certificate of Analysis Minimum Reporting Limit 1.0 PO#: Receipt: 11/11/22 10:45@ 0.3 °C Date Reported: 12/2/2022 Project Name: November Ground Water 2022 Sampled By: Tanner Holliday Method EPA 8260D 15030A CtF WO#: 22K0963 Preparation Date/Time 11/16/22 Lab ID: 22K0963-07 Analysis Date/Time 11/16/22 .E!.J!g{fil Page 9 of 18 9632 South 500 West CHEMTECH·FORD LABOR/\T0 ~ IE S 12/2/2022 Work Order: 22K0963 Project: November Ground Water 2022 Energy Fuels Resources, Inc. Attn: Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Client Service Contact: 801.262. 7299 The analyses presented on this report were performed in accordance with the National Environmental Laboratory Accreditation Program (NELAP) unless noted in the comments, flags, or case narrative. If the report is to be used for regulatory compliance, it should be presented in its entirety, and not be altered. Approved By: Melissa Connolly, Project Manager Sandy, Utah 84070 801.262.7299 Main 866.792.0093 Fax Serving the lntermountain West since 1953 www.ChemtechFord.com Page 1 of 18 CH EM TECH-FORD LABOAATORIES Energy Fuels Resources, Inc. Project: November Ground Water 2022 Project Manager: Tanner Holliday Laboratory ID 22K0963-01 22K0963-02 22K0963-03 22K0963-04 22K0963-05 22K0963-06 22K0963-07 Sample Name MW-11 _11082022 MW-25_ 11092022 MW-26_ 11102022 MW-30_ 11092022 MW-31_11082022 MW-65_ 11092022 Trip Blank Work Order Report Narrative Sample Preparation All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions There are no corrective actions associated with this work order. Project Name: November Ground Water 2022 www.ChemtechFord.com CtF WO#: 22K0963 Page 2 of 18 I CHEMTECH-FORD LABORATORIES Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations Certificate of Analysis PO#: Receipt: 11/11/22 10:45@ 0.3 °C Date Reported: 12/2/2022 Project Name: November Ground Water 2022 ND= Not detected at the corresponding Minimum Reporting Limit (MRL). I mg/L = one milligram per liter or I mg/kg= one milligram per kilogram = I part per million. I ug/L = one microgram per liter or I ug/kg = one microgram per kilogram= I part per billion. I ng/L = one nanogram per liter or I ng/kg = one nano gram per kilogram = I part per trillion. Flag Descriptions QM-4X = The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to anaJyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Project Name: November Ground Water 2022 www.ChemtechFord.com CtF WO#: 22K0963 Page 10 of 18 8 I 10 ,2 I Address: Contact: Phone#: Email: Project Name: Project#: PO#: Sampler Name: 2..1-/ic1o/Co'J IIIW-11_11082022 IIIW-25_11092022 IIIW-26_11102022 IIIW-30_11092022 MW-31_11082022 MW-65_11092022 Trip Blank American West Analytical Laboratories 463 W. 3600 S. Salt Lake City, UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 1 6425 8. Hwy. 191 Blanding, UT 84511 Tanner Holliday (435) 678-2221 Cell#: thoWda:,@;eDerDfaeb.com; lr:welne~erir;yfaels.com; November Ground Water 2022 Tanner Holliday Samele ID: Date SamDled 11/8/2022 11/9/2022 11/10/2022 11/9/2022 11/8/2022 11/9/2022 11/10/2022 Rellnqulohedb!:.:J JL.// .. L __ Oete: Sln~eturo I tu1 n I If._ ,,,1012022 I/ llme: PrtnlName: Tanner Ho.l.lida" 1130 Re11nqu1ened by: Date: Sklneh..ire Tlme: PrtnlName; Rollnqulehed by: Date Sionature Time: Print Name: Rellnqulehed by: Dale: Slaneture Time: Print Name: CHAIN OF CUSTODY All analysis wlll be conducted using NELAP accredited methods and all data wlll be reported using AWAL'e standard enalyte llsta and reporting llmlls (PQL) unlesa speciflcally requested otherwise on this Chain or Custody and/or attached documentation. AWAL Lab Sample Set# Page of I QC Level: I Turn Around Time: Unless other arrangemenlB have been made, r•DAfo stgned reports wlll be emeUed by 5:00 pm on 3 Standard the day they are due. I X Include EDD: Laboratory Use Only LOCUS UPLOAD EXCEL Sample-, Wor•· I.AP5 X Field Filtered For: Dlaaolved lllletala , Shlpp<>d or •nd dollv0tod 00 co' A anlE) ci 00 co' co' 0 2 0 ci 0 0 0 For Compliance With: IN c::, c::, C'I Tamp<Maturo CJ • .? ·c ..._ 0 C'I C'I ;:::. D NELAP a [',, IN ;:::. ;:::. ci ..._ 0 Q' D RCRA 0 [',, 0 0 c::, D CWA 4 Received Broken/Leaking £!. ci c::, ~ c::, c::, IO D SOWA (Improperly Sealed) 0 ~ ~ C'I I £!. I i 9 ~ D ELAP/A2LA y N u 9 u o' D NLLAP ~ o' ! c:i B C'i' Ill 0 l i! c::, D Non-Compliance 5 Property Preserved ~ ~ c::, "II .!l ~ O') ,2 D Other: y N O') II dl ... 0 Checked et bench I!! !!l. :a ... G' u :a 0 .. ID X 0 c::, c::, ~ y N ·c Cf) "II "II "Cl "Cl "II C .; c::, ;'J; c::, s i .E u " u u It) ::; c::, ~ ~ ~ ~ lit. u Known Hazards 6 Received Within C It) £!. 8 ID -: lit. : : : : ~ c!Sngllmee Time a. (II al • & 'o E 0 u ~ 5l g . N Samoled .. ~ II!: i5 i5 i5 i5 i5 Samele Comments 1230 4 w X X X X X 17_,v-";l.._ 7(.' l'V! I Z l/ (i-_ 1110 I w X /1, /'J...-71-- 715 5 w X X X g·~~-,-Y N NA 1035 3 w X X X X ..,_JC'?) I :ll.. C -~ 2 . cm on Outer Package 1420 4 w X, x-x · X x · • Y N NA 1035 3 w X X X X 3 Pteon, on Sample E) y N 4 Unbro~an on Somi,lo 8 715 3 w X Y N NA Dlacrvpanclea Betw9en Semple y N Labels and COC Recob Received by: Date: Special Instructions: Signature [Tlme: PrtntNema: / Sample containers for metals were field filtered. See the RooolY~ ~ (f_k._., __/ D•7i ///7z.. i..--Analytical Scope of Work for Reporting Limits and voe analyte ;Slonoturo -f. ,:,vz,.,......_ P,lnl Nomo: £ /4,, '--1-1,:V"!;.1 a.._~/ / 1101itil/S list. ~· --·· ·--1 .•.• Received by: I Data: l'/.187Y4YU:W6071855 I Slonelure Nov 11 !c:11:'.iQl:cl':l ZQ1ZZ [Tlme: 182?7L9 HIPP~j . ' Print Name: Received lly: Oete: $1onelure I Page 11 of 18 Time: IPrtr,tNeme: Analyte QC Sample ID: BWK092 l-BLK1 Date Prepared: 11/21/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWK0921-BS1 Date Prepared: 11/21/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWK0921-MS1 Date Prepared: I 1/21/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWK0921-MS2 Date Prepared: 11/21/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved QC Sample ID: BWK0921-MS3 Date Prepared: 11/21/2022 Manganese, Dissolved Selenium, Dissolved Uranium, Dissolved CtF WO#: 22K0963 www.ChemtechFord.com QC Report for Work Order (WO) -22K0963 % Rec RPD Limits RPD Max Result Source Cone SpkValue MRL DF Blank -EPA 200.8 Batch: BWK092 l Date Analyzed: 11/21/2022 Units: mg/L ND 0.0100 1.00 ND 0.0050 1.00 ND 0.0003 1.00 LCS -EPA 200.8 Batch: BWK0921 Date Analyzed: 11/21/2022 Units: mg/L 109 85 -115 0.044 0.D400 0.0005 1.00 104 85 -115 0.042 0.0400 0.0005 1.00 105 85 -115 0.042 0.0400 0.0003 1.00 Matrix Spike -EPA 200.8 Batch: BWK0921 QC Source Sample: 22K0963-0l Date Analyzed: 11/21/2022 Units: mg/L 106 70 -130 0.263 0.220 0.0400 0.0005 1.00 121 70 -130 0.067 0.019 0.0400 0.0005 1.00 103 70 -130 0.044 0.002 0.0400 0.0003 1.00 Batch: BWK0921 QC Source Sample: 22K0963-06 Date Analyzed: 11/21/2022 Units: mg/L 104 70 -130 0.048 0.006 0.0400 0.0005 1.00 115 70-130 0.123 0.077 0.0400 0.0005 1.00 103 70 -130 0.052 0.010 0.0400 0.0003 1.00 Batch: BWK0921 QC Source Sample: XXXXXXX-XX Date Analyzed: ll /21/2022 Units: mg/L 92.6 70 -130 0.116 0.079 0.0400 0.0005 1.00 105 70 -130 0.042 0.0002 0.0400 0.0005 1.00 104 70 -130 0.042 0.0009 0.0400 0.0003 1.00 Page 12 of 18 QC Report for Work Order (WO) -22K0963 Analyte %Rec RPO Limits RPO Max Result Source Cone SpkValue MRL OF Blank -EPA 300.0 QC Sample ID: BWK.0546-BLKI Batch: BWK.0546 Date Prepared: 11/11/2022 Date Analyzed: 11/14/2022 Units: mg/L Sulfate ND 1.00 1.00 QC Sample ID: BWK0674-BLK1 Batch: BWK0674 Date Prepared: 11/15/2022 Date Analyzed: 11/16/2022 Units: mg/L Chloride ND 1.00 1.00 QC Sample ID: BWK.0750-BLKl Batch: BWK.0750 Date Prepared: 11/16/2022 Date Analyzed: 11/17/2022 Units: mg/L Chloride ND 1.00 1.00 QC Sample ID: BWKl 114-BLKl Batch: BWK1114 Date Prepared: 11/28/2022 Date Analyzed: 11/29/2022 Units: mg/L Sulfate ND 1.00 1.00 LCS -EPA 300.0 QC Sample ID: BWK.0546-BSl Batch: BWK.0546 Date Prepared: 11/11/2022 Date Analyzed: 11/14/2022 Units: mg/L Sulfate 92.6 90 -110 46.3 50.0 1.00 1.00 QC Sample ID: BWK0674-BS1 Batch: BWK.0674 Date Prepared: 11 /15/2022 Date Analyzed: 11/16/2022 Units: mg/L Chloride 99.2 90-110 49.6 50.0 1.00 1.00 QC Sample ID: BWK.0750-BSl Batch: BWK.0750 Date Prepared: 11/16/2022 Date Analyzed: 11/17/2022 Units: mg/L Chloride 101 90 -110 50.6 50.0 1.00 1.00 QC Sample ID: BWK1114-BS1 Batch: BWK1114 Date Prepared: 11/28/2022 Date Analyzed: 11/29/2022 Units: mg/L Sulfate 101 90 -110 50.7 50.0 1.00 1.00 Matrix Spike -EPA 300.0 QC Sample ID: BWK.0546-MSl Batch: BWK.0546 QC Source Sample: XXXXXXX-XX Date Prepared: 11/11/2022 Date Analyzed: 11/14/2022 Units: mg/L Sulfate 103 80 -120 2650 2130 500 55.0 1.00 QC Sample ID: BWK0546-MS2 Batch: BWK.0546 QC Source Sample: 22K0963-01 Date Prepared: 11/11/2022 Date Analyzed: 11/14/2022 Units: mg/L Chloride 82.2 80 -120 461 50.3 500 55.0 1.00 Sulfate 98.4 80 -120 1630 1140 500 55.0 1.00 QC Sample ID: BWK0674-MS1 Batch: BWK.0674 QC Source Sample: XXXXXXX-XX Date Prepared: 11/15/2022 Date Analyzed: 11/16/2022 Units: mg/L Chloride -6090 80 -120 769 6860 100 11.0 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWK0674-MS2 Batch: BWK.0674 QC Source Sample: 22K0963-0l Date Prepared: 11/15/2022 Date Analyzed: 11/16/2022 Units: mg/L Chloride 79.9 80 -120 80.8 71 .9 11.1 1.11 1.00 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWK0674-MS3 Batch: BWK.0674 QC Source Sample: 22K0963-03 Date Prepared: 11/15/2022 Date Analyzed: 11/16/2022 Units: mg/L Chloride 78.6 80 -120 68.0 59.2 11.1 1.11 1.00 CtF WO#: 22K0963 www.ChemtechFord.com Page 13 of 18 QC Report for Work Order (WO) -22K0963 Analyte % Rec RPO Limits RPO Max Result Source Cone Matrix Spike -EPA 300.0 (cont.) QC Sample ID: BWK0674-MS3 Batch: BWK0674 QC Source Sample: 22K0963-03 Date Prepared: 11/15/2022 Date Analyzed: 11/16/2022 Units: mg/L QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWK0674-MS4 Batch: BWK.0674 QC Source Sample: 22K0963-06 Date Prepared: 11/15/2022 Date Analyzed: 11/16/2022 Units: mg/L Chloride 92.8 80 -120 229 183 QC Sample ID: BWK0750-MS 1 Batch: BWK.0750 QC Source Sample: XXXXXXX-XX Date Prepared: 1 l /16/2022 Date Analyzed: 11/17/2022 Units: mg/L Chloride 465 80 -120 51.6 QC Sample ID: BWK.1114-MSl Batch: BWK.1114 QC Source Sample: XXXXXXX-XX Date Prepared: 11/28/2022 Date Analyzed: 11/29/2022 Units: mg/L Sulfate 72.5 80 -120 1220 1150 Matrix Spike Dup -EPA 300.0 QC Sample ID: BWK.0546-MSDI Batch: BWK0546 QC Source Sample: XXXXXXX-XX Date Prepared: 11/11/2022 Date Analyzed: 11/14/2022 Units: mg/L Sulfate 103 0.00711 80 -120 20 2650 2130 QC Sample ID: BWK0546-MSD2 Batch: BWK.0546 QC Source Sample: 22K0963-0l Date Prepared: 11/11/2022 Date Analyzed: 11/15/2022 Units: mg/L Sulfate 98.2 0.0530 80 -120 20 1630 1140 QC Sample ID: BWK.0674-MSDl Batch: BWK0674 QC Source Sample: XXXXXXX-XX Date Prepared: 1 l /15/2022 Date Analyzed: 11/16/2022 Units: mg/L Chloride -6090 0.289 80 -120 20 767 6860 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWK0674-MSD2 Batch: BWK.0674 QC Source Sample: 22K0963-0l Date Prepared: 11/15/2022 Date Analyzed: 11/16/2022 Units: mg/L Chloride 74.2 0.788 80 -120 20 80.2 71.9 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. QC Sample ID: BWK0674-MSD3 Batch: BWK0674 QC Source Sample: 22K0963-03 Date Prepared: 11/15/2022 Date Analyzed: 1 I /16/2022 Units: mg/L Chloride 86.8 1.33 80 -120 20 68.9 59.2 QC Sample ID: BWK0674-MSD4 Batch: BWK.0674 QC Source Sample: 22K0963-06 Date Prepared: 11/15/2022 Date Analyzed: 11/16/2022 Units: mg/L Chloride 87.6 1.15 80 -120 20 227 183 QC Sample ID: BWK.0750-MSDI Batch: BWK0750 QC Source Sample: XXXXXXX-XX Date Prepared: 11/16/2022 Date Analyzed: 11/17/2022 Units: mg/L Chloride 465 0.0807 80 -120 20 51.7 QC Sample ID: BWK.1114-MSDI Batch: BWK.1114 QC Source Sample: XXXXXXX-XX Date Prepared: 11/28/2022 Date Analyzed: 11/29/2022 Units: mg/L Sulfate 82.3 0.794 80 -120 20 1230 1150 CtF WO#: 22K0963 www.ChemtechFord.com Spk Value MRL OF 50.0 5.50 1.00 11.1 1.11 1.00 100 11.0 1.00 500 55.0 1.00 500 55.0 1.00 100 11.0 1.00 11.1 1.11 1.00 11.1 1.11 1.00 50.0 5.50 1.00 11.1 1.11 1.00 100 11.0 1.00 Page 14 of 18 Analyte QC Sample ID: BWK0909-BLK1 Date Prepared: l l/21/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWK0909-BS1 Date Prepared: 11/21/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: B WK0909-MS 1 Date Prepared: l l /21/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWK0909-MS2 Date Prepared: 11/21/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWK0909-MS3 Date Prepared: 11 /2 1/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWK0909-MS4 Date Prepared: 11/21/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWK0909-MSDI Date Prepared: l 1/2 l /2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWK0909-MSD2 Date Prepared: 11/21/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWK0909-MSD3 Date Prepared: 11/21/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWK0909-MSD4 Date Prepared: 11/21/2022 Nitrate + Nitrite, Total, as N CtF WO#: 22K0963 www. Chem tech Ford. com QC Report for Work Order (WO) -22K0963 %Rec RPD Limits RPD Max Result Source Cone Blank -EPA 353.2 Batch: BWK0909 Date Analyzed: 11 /21/2022 Units: mg/L ND LCS -EPA 353.2 Batch: BWK0909 Date Analyzed: 11/21/2022 Units: mg/L 94.7 80 -120 1.89 Matrix Spike -EPA 353.2 Batch: BWK0909 QC Source Sample: XXXXXXX-XX Date Analyzed: 11 /2 I /2022 Units: mg/L 93.7 80 -120 9.65 8.71 Batch: BWK0909 QC Source Sample: 22K0963-0l Date Analyzed: 1 l /2 I /2022 Units: mg/L 102 80 -120 3.76 2.74 Batch: BWK0909 QC Source Sample: 22K0963-03 Date Analyzed: 11/21/2022 Units: mg/L 92.1 80 -120 1.33 0.408 Batch: BWK0909 QC Source Sample: 22K0963-06 Date Analyzed: 11/21/2022 Units: mg/L 101 80 -120 16.7 15.7 Matrix Spike Dup -EPA 353.2 Batch: BWK0909 QC Source Sample: XXXXXXX-XX Date Analyzed: l l /2 l /2022 Units: mg/L 97.7 0.414 80 -120 20 9.69 8.71 Batch: BWK0909 QC Source Sample: 22K0963-0I Date Analyzed: ll /21 /2022 Units: mg/L 101 0.267 80 -120 20 3.75 2.74 Batch: BWK0909 QC Source Sample: 22K0963-03 Date Analyzed: l l /2 l /2022 Units: mg/L 87.6 3.44 80 -120 20 1.28 0.408 Batch: BWK0909 QC Source Sample: 22K0963-06 Date Analyzed: 11/21/2022 Units: mg/L 105 0.191 80 -120 20 16.8 15.7 Spk Value MRL DF 0.100 1.00 2.00 0.100 1.00 1.00 0.500 5.00 1.00 0.100 1.00 1.00 0.100 1.00 1.00 0.500 5.00 1.00 0.500 5.00 1.00 0.100 1.00 1.00 0.100 1.00 1.00 0.500 5.00 Page 15 of 18 QC Report for Work Order (WO) -22K0963 Analyte %Rec RPO Limits RPO Max Result Source Cone Blank -EPA 8260D /5030A QC Sample ID: BWK0760-BLK1 Batch: BWK0760 Date Prepared: 11/16/2022 Date Analyzed: 11/16/2022 Units: Chloroform ND LCS -EPA 8260D /5030A QC Sample ID: BWK0760-BS1 Batch: BWK0760 Date Prepared: 11/16/2022 Date Analyzed: 11/16/2022 Units: Chloroform 104 70 -130 10.4 Matrix Spike -EPA 8260D /5030A QC Sample ID: BWK0760-MS1 Batch: BWK0760 QC Source Sample: 22K0963-03 Date Prepared: 11/16/2022 Date Analyzed: 11/16/2022 Units: Chloroform -3920 70 -130 120 512 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Matrix Spike Dup -EPA 8260D /5030A QC Sample ID: BWK0760-MSD1 Batch: BWK0760 QC Source Sample: 22K0963-03 Date Prepared: 11/16/2022 Date Analyzed: 11/16/2022 Units: Chloroform -4030 -2.68 70 -130 20 110 512 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. CtF WO#: 22K0963 www.ChemtechFord.com ug/L ug/L ug/L ug/L SpkValue MRL OF 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 10.0 1.0 1.00 Page 16 of 18 Analyte QC Sample ID: BWK0545-BLK1 Date Prepared: 11/11 /2022 Total Dissolved Solids (TDS) QC Sample ID: BWK0591-BLK1 Date Prepared: 11/14/2022 Total Dissolved Solids (TDS) QC Sample ID: BWK0545-DUP1 Date Prepared: 11/11/2022 Total Dissolved Solids (TDS) QC Sample ID: BWK0545-DUP2 Date Prepared: 11/11/2022 Total Dissolved Solids (TDS) QC Sample ID: BWK0591-DUP1 Date Prepared: 11/14/2022 Total Dissolved Solids (TDS) QC Sample ID: BWK0591-DUP2 Date Prepared: 11/14/2022 Total Dissolved Solids (TDS) QC Sample ID: BWK0545-BSI Date Prepared: 11/11/2022 Total Dissolved Solids (TDS) QC Sample ID: BWK0591-BS1 Date Prepared: 11/14/2022 Total Dissolved Solids (TDS) CtF WO#: 22K0963 www.ChemtechFord.com QC Report for Work Order (WO) -22K0963 % Rec RPD Limits RPD Max Result Source Cone Spk Value MRL DF Blank -SM 2540 C Batch: BWK0545 Date Analyzed: 11/11/2022 Units: mg/L ND 10 1.00 Batch: BWK0591 Date Analyzed: 11/14/2022 Units: mg/L ND 10 1.00 Duplicate -SM 2540 C Batch: BWK0545 QC Source Sample: XXXXXXX-XX Date Analyzed: 11/11/2022 Units: mg/L 0.2 10 1920 1920 20 1.00 Batch: BWK0545 QC Source Sample: 22K0963-0l Date Analyzed: 11/11/2022 Units: mg/L 10 2300 2270 20 1.00 Batch: BWK0591 QC Source Sample: XXXXXXX-XX Date Analyzed: 11/14/2022 Units: mg/L 10 296 300 20 1.00 Batch: BWK0591 QC Source Sample: XXXXXXX-XX Date Analyzed: 11/14/2022 Units: mg/L 10 288 284 20 1.00 LCS -SM 2540 C Batch: BWK0545 Date Analyzed: 11/11/2022 Units: mg/L 100 90 -110 400 400 20 1.00 Batch: BWK0591 Date Analyzed: 11/14/2022 Units: mg/L 104 90 -110 416 400 20 1.00 Page 17 of 18 Surrogates Report for Work Order (WO) -22K0963 QCID Analyte % Rec LCL UCL Result SpkValue Blank -EPA 8260D /5030A BWK0760-BLK1 1,2-Dichloroethane-d4 100 64.2 126 10.0 10.0 BWK0760-BLK1 4-Bromofluorobenzene 97.9 71.4 125 9.79 10.0 BWK0760-BLK1 Toluene-dB 98.3 63.2 129 9.83 10.0 LCS -EPA 8260D /5030A BWK0760-BS1 1,2-Dichloroethane-d4 97.7 64.2 126 9.77 10.0 BWK0760-BS1 4-Bromofluorobenzene 97.5 71.4 125 9.75 10.0 BWK0760-BS1 Toluene-dB 100 63.2 129 10.0 10.0 Matrix Spike -EPA 8260D /5030A BWK0760-MS1 1,2-Dichloroethane-d4 102 64.2 126 10.2 10.0 BWK0760-MS1 4-Bromofluorobenzene 98.8 71.4 125 9.88 10.0 BWK0760-MS1 Toluene-dB 100 63.2 129 10.0 10.0 Matrix Spike Dup -EPA 8260D /5030A BWK0760-MSD1 1,2-Dichloroethane-d4 99.3 64.2 126 9.93 10.0 BWK0760-MSD1 4-Bromofluorobenzene 97.1 71.4 125 9.71 10.0 BWK0760-MSD1 Toluene-dB 100 63.2 129 10.0 10.0 Surrogate Recoveries (Field Samples) LabNumber Analyte Result Spklvl %Rec LCL UCL 8260 Low Level Volatiles 22K0963-03 Toluene-dB 22K0963-03 4-Bromofluorobenzene 22K0963-03 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22K0963-07 Toluene-dB 22K0963-07 22K0963-07 4-Bromofluorobenzene 1,2-Dichloroethane-d4 CtF WO#: 22K0963 www.ChemtechFord.com 10.1 9.92 9.98 9.93 9.75 9.57 10.0 10.0 10.0 10.0 10.0 10.0 101 99.2 99.8 99.3 97.5 95.7 63.2 129 71.4 125 64.2 126 63.2 129 71.4 125 64.2 126 Batch DF BWK0760 1.00 BWK0760 1.00 BWK0760 1.00 BWK0760 1.00 BWK0760 1.00 BWK0760 1.00 BWK0760 1.00 BWK0760 1.00 BWK0760 1.00 BWK0760 1.00 BWK0760 1.00 BWK0760 1.00 Qualifier Page18of18 TabF2 Laboratory Analytical Reports -Accelerated Monitoring December 2022 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com Serving the lntermountain West Since 1953 CHEMTECH-FORD LABORATOrues Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-11_12142022 Matrix: Water Date Sampled: 12/14/22 12:15 Inorganic Chloride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \lctals Manganese, Dissolved Result 52.3 1.30 1330 2370 0.273 Proiect Name: December Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 1.00 0.l00 20.0 20 0.0100 PO#: Receipt: 12/16/22 8:44@ -0.1 °C Date Reported: 1/3/2023 Project Name: December Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 EPA300.0 SM2540C EPA200.8 CtF WO#: 22L 1318 Preparation Date/Time 12/28/22 12/16/22 12/19/22 12/16/22 12/20/22 Lab ID: 22L1318-01 Analysis Date/Time 12/29/22 12/16/22 12/19/22 12/16/22 12/20/22 f!..!!lru). Page 3 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD LA80AA'r0RleS Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-25_12142022 Matrix: Water Date Sampled: 12/14/22 11 :45 Inorganic Total Dissolved Solids (TDS) Result 2780 Proiect Name: December Ground Water 2022 www.ChemtechFord.com Units mg/L Certificate of Analysis Minimum Reporting Limit 20 PO#: Receipt: 12/16/22 8:44@ -0.1 °C Date Reported: 1/3/2023 Project Name: December Ground Water 2022 Sampled By: Tanner Holliday Method SM 2540 C CtF WO#: 22L 1318 Preparation Date/Time 12/16/22 Lab ID: 22Ll318-02 Analysis Date/Time 12/16/22 I!J!.g{fil Page 4 of 20 Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD tAEIOAAlOAll:S Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-26_12152022 Matrix: Water Date Sampled: 12/15/22 8:00 Inorganic Chloride Nitrate+ Nitrite, Total, as N \'olatilc Organic Compounds Chloroform Result 60.6 2.66 460 Proiect Name: December Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L ug/L Certificate of Analysis Minimum Reporting Limit 1.00 0.100 100 PO#: Receipt: 12/16/22 8:44@ -0.1 °C Date Reported: 1/3/2023 Project Name: December Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 EPA 8260D /5030A CtF WO#: 22L 1318 Preparation Date/Time 12/28/22 12/16/22 12/19/22 Lab ID: 22Ll318-03 Analysis Date/Time 12/29/22 12/16/22 12/19/22 Page 5 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www. Chem tech Ford. com Serving the lntermountain West Since 1953 CHEMTECH-FORD LABOIIATORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-30_12132022 Matrix: Water Date Sampled: 12/13/22 12:25 Inorganic Chloride Nitrate+ Nitrite, Total, as N \lctals Selenium, Dissolved Uranium, Dissolved Result 195 16.1 0.0708 0,0130 Proiect Name: December Ground Water 2022 www. Chem tech Ford. com Units mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 5.00 0.500 0.0050 0.0003 PO#: Receipt: 12/16/22 8:44@ -0.1 °C Date Reported: 1/3/2023 Project Name: December Ground Water 2022 Sampled By: Tanner Holliday EPA300.0 EPA353.2 EPA200.8 EPA200.8 CtF WO#: 22L1318 Preparation Date/Time 12/28/22 12/29/22 12/20/22 12/20/22 Lab ID: 22L1318-04 Analysis Date/Time 12/29/22 12/29/22 12/20/22 12/20/22 .E!J!g(tl Page 6 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0:(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD lABOAAt'ORIES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-31_12132022 Matrix: Water Date Sampled: 12/13/22 14:25 Inorganic Chloride Nitrate+ Nitrite, Total, as N Sulfate Total Dissolved Solids (TDS) \lctals Uranium, Dissolved 335 12.6 1280 2700 0.0262 Proiect Name: December Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 5.00 0.500 20.0 20 0.0003 PO#: Receipt: 12/16/22 8:44 @ -0.1 °C Date Reported: 1/3/2023 Project Name: December Ground Water 2022 Sampled By: Tanner Holliday Method EPA300.0 EPA353.2 EPA300.0 SM 2540 C EPA200.8 CtF WO#: 22L1318 Preparation Date/Time 12/28/22 12/16/22 12/19/22 12/16/22 12/20/22 Lab ID: 22L1318-05 Analysis Date/Time 12/29/22 12/16/22 12/19/22 12/16/22 12/20/22 .El!lilll Page 7 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORO lA80JIAT0~1E$ Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: MW-65_12132022 Matrix: Water Date Sampled: 12113122 12:25 Inorganic Chloride Nitrate+ Nitrite, Total, as N \lctals Selenium, Dissolved Uranium, Dissolved Result 183 15.2 0.0780 0.0126 Proiect Name: December Ground Water 2022 www.ChemtechFord.com Units mg/L mg/L mg/L mg/L Certificate of Analysis Minimum Reporting Limit 5.00 0.500 0.0050 0.0003 PO#: Receipt: 12116122 8:44@ -0.1 ·c Date Reported: 1/3/2023 Project Name: December Ground Water 2022 Sampled By: Tanner Holliday EPA300.0 EPA353.2 EPA200.8 EPA200.8 CtF WO#: 22L 1318 Preparation Date/Time 12/28/22 12/16/22 12/20/22 12/20/22 Lab ID: 22L1318-06 Analysis Date/Time 12/29/22 12/16/22 12/20/22 12/20/22 fug{fil Page 8 of 20 I Chemtech-Ford Laboratories 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Serving the lntermountain West Since 1953 CHEMTECH-FORD LA90flAYOA:IES Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Sample ID: Trip Blank Matrix: Water Date Sampled: 12/15/22 8:00 \'olatilc Or~anic Compounds Chloroform < 1.0 Proiect Name: December Ground Water 2022 www.ChemtechFord.com Units ug/L Certificate of Analysis Minimum Reporting Limit 1.0 PO#: Receipt: 12/16/22 8:44@ -0.1 °C Date Reported: 1/3/2023 Project Name: December Ground Water 2022 Sampled By: Tanner Holliday Method EPA 8260D 15030A CtF WO#: 22L 1318 Preparation Date/Time 12/19/22 Lab ID: 22L1318-07 Analysis Date/Time 12/19/22 fug{fil Page 9 of 20 9632 South 500 West I CHEMTECH·FORD l.A D O~.oHOi! IIES 1/3/2023 Work Order: 22L1318 Project: December Ground Water 2022 Energy Fuels Resources, Inc. Attn: Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Client Service Contact: 801.262.7299 The analyses presented on this report were performed in accordance with the National Environmental Laboratory Accreditation Program (NELAP) unless noted in the comments, flags, or case narrative. If the report is to be used for regulatory compliance, it should be presented in its entirety, and not be altered. Approved By: Melissa Connolly, Project Manager Sandy, Utah 84070 801.262.7299 Main 866.792.0093 Fax Serving the lntermountain West since 1953 www.ChemtechFord.com Page 1 of 20 I CHEMTECH-FORD LAB051AT0F!:IE:S Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Energy Fuels Resources, Inc. Project: December Ground Water 2022 Project Manager: Tanner Holliday Laboratory ID 22L1318-01 22L 1318-02 22L 1318-03 22L1318-04 22L 1318-05 22L 1318-06 22L 1318-07 Sample Name MW-11 _ 12142022 MW-25_ 12142022 MW-26_ 12152022 MW-30 _ 12132022 MW-31_ 12132022 MW-65 _ 12132022 Trip Blank Sample Preparation Work Order Report Narrative All samples were prepared within method specified holding times. No preparation issues were noted. Method Blanks All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any analysis in this work order. Laboratory Control Samples All laboratory control samples were within method acceptance criteria. Method Spikes All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags. Method Spike Duplicates All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags. Corrective Actions There are no corrective actions associated with this work order. Page 2 of 20 CHEMTECH-FORD LABORATO~IES Chemtech-Ford Laboratories Serving the lntermountain West Since 1953 9632 South 500 West Sandy, UT 84070 0 :(801) 262-7299 F: (866) 792-0093 www.ChemtechFord.com Certificate of Analysis Energy Fuels Resources, Inc. Tanner Holliday 6425 South Highway 191 Blanding, UT 84511 Report Footnotes Abbreviations ND= Not detected at the corresponding Minimum Reporting Limit (MRL). PO#: Receipt: 12/16/22 8:44@ -0.1 °C Date Reported: 1/3/2023 Project Name: December Ground Water 2022 I mg/L = one milligram per liter or I mg/kg= one milligram per kilogram = 1 part per million, 1 ug/L = one microgram per liter or I ug/kg = one microgram per kilogram= I part per billion. I ng/L = one nano gram per liter or I ng/kg = one nanogram per kilogram = I part per trillion. Proiect Name: December Ground Water 2022 www.ChemtechFord.com CtF WO#: 22L1318 Page 10 of 20 I, i ~ r'4 'S ~ '\ I I ! I American West '1,,ZA . .,{ '?ltAnalytical Laboratories 463 W. 3600 S. Sall Lake City, UT 84115 Phone# (801) 263-8686 Toll Free # (888) 263-8686 L~ Fax# (801) 263-8687 Email awal@awal-labs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 8. Hwy. 191 Blanding, UT 84511 Contact: Tanner Holliday Phone#: (4351 678-2221 Cell#: Email: tholllda:,@enerc,faela.com; kweiDeJ@enerafaela.com; Project Name: December Ground Water 2022 Project#: PO#: Sampler Name: Tanner Holliday . SamDle ID: Date SamDled IIW-11_12142022 12/14/2022 IIW-25_12142022 12/14/2022 IIW-26_12152022 12/15/2022 IIW-30_12132022 12/13/2022 IIW-31_12132022 12/13/2022 IIW-65_12132022 12/13/2022 Trip Blank 12/15/2022 Rellr>qlli.ohed b:::) J,JJ L ,_/_ Oate: Slanorure In A••• 12/15/2022 V Tlme: Print Name: Tanner Hollldav 1100 Relinquished by: Dale: $1g"81ure Time: Print Name,.: Reffnqul8hed by: Date: SJanahl"' Time: PrlntName; Reffnquhlhed by: Date: Slonalure Time: Print Name: CHAIN OF CUSTODY All analysis ¥1411 be conducted using NELAP accredited methods and all dela will be reported using AWAL's standard anaryte llsts and reporting limits {POL) unless specfRcalfy requaated otherMse on this Chain or Custody and/or attached documenlatk>n. AWAL Lab Sample Sel # Page of QC Level: Tum Around Time: Unl8S8 other arrangement& have been made, I°"' Da<e ~ olgned reportll will be emailed by 5:00 pm on Standard the day lhey are due. - X Include EDD: Laboratory Use Only LOCUS UPLOAD EXCEL Sample& W6f8: X Field Filtered For: Dl.uohred Metala 1 Shipped or hand dollv6f8d 00 ~ ~ c:i 00 ~ c:i 2 Ambient or Chilled 0 c:i c:i c:i c::, For Compliance With: Temperature -6. I C'I c::, c::, c-. ----0 c-. c-. ;::: □ NELAP 3 ·c t'-C'I ;::: ;::: c:i ----c:i i:i' □ RCRA 0 t'-c:i c:i c::, □ CWA £!. c:i c::, c::, ~ c::, 4 ROCGived Brokon/1.oaklng 0 IC) D SOWA = C'I ~ C:!. .. c-. (Improperly Sealed) -] 9 • ~ □ ELAP/ A2LA y N u 9 .. o' D NLLAP ~ ! o' i! t c:i e □ Non-Compliance c:i ] a c::, 5 Property Preaerved ~ ~ c::, .,, .!! "l .s □ Other: y N "l ~ iJl .. 0 ; !!2. lll .. G' lll 0 .. Chocked al bench :s 0 c::, c::, 0 y N C: C'l .,, c::, ;J; .,, .,, .,, .,, c::, :a j :J 0 .. u .. u ! .!: c::, .!: .!: .!: "' u Known Hazards 6 Racetvad Wllhln II: "' ~ :t. .. ..... a :t. a 0 a a i Holding 11meo Time ci. N ! = .. & 0 E i a i y N SamDled .. c1l i5 i5 i5 i5 i5 SamDle Comments 1215 4 w X X X X X 1145 I w X 800 5 w X X X 1 Preeant on Outa, Package y N NA 1225 3 w X X X X 2 Unbroken on Outer Package 1425 4 w X X X X X y N NA 1225 3 w X X X X 3 Present on Sample y N NA 4 Unbroken on Sample 800 3 w X y N NA OIKtoPAndoo Ba_, Sample 1ll1111111 II''""' ........ 7 ( A 0(. 1Z187Y4Y0392186926 V vi - Racetvod ~ / y ,,..../ c:..1,,inature I),,/ A ~ .J.,.. ~ Oot•:n •• / \p-7-1-Special Instructions: ..__..v . 11mo; Q ~ L\ 4 Print Name: Sample containers for metals were field filtered. See the Received by: Date: SJonalure Analytical Scope of Work for Reporting Limits and voe analyte Tlma: 1:- PrlnlNAmo: Received by: Doto: Sample Receipt Conditions: Slanalur8 /) Custody Seals Present vf COrrect Containers ( ) Headspace Present (VOC) Timo: /I COC Included ( ) Temperature Blank PrinlNama: Y, Containers Intact t~ece1ved within Hold Racetved by: D•to: COC and t..ib<:ls Match Sla'l8lur9 Sufficient Sample Volume Ct,ock4!d bv: I 1=" I ,0' COC Complete Y, Rec.?1ved on Ice Timo: Page 11 of 20 PrintN■m■: - Work Order# 1,;~L l~l9:) ------- Delivery Method: /uPs d ' _ .. ; --~ . Sam_ple# -D\ ~CA· (f':J -t71- b3 n'A ~ r ~\\/ ('YO~ \ .~, 10;:;1" l)'P " 01 D USPS h I hC Container An (7..) W\ N A10 Pnn N W{J) Lt tJ Pr-a ~ ™ v'I\ N 'v0 (~') ouner j .• t rnrier I , I i i I I I Chemtech Lot • i .& '5 ~1 ar ] Preservative i " 17_30 \-7 uo... i -Z...,'3--Z.. l'7.~n J'2?D JZ-3'2. l'l-35 \'7,:;,i l '1--~ 11 ... u Cb \--Z..~O o)-1\& \1 ... :-Z,Z.. f,Z,.'3S- ~ ~ I Misc ; Ji I Volume I (oz/ml) CHEMTECH FORD LABORATORIES Sample Receipt Receiving Temperature -0 · \ ·c I_;-• •· ). t.'°1~'-, -~ ..a1...-. ~~1::....:.1 1,. -,. ~. ·.a ~ • • ... ·~-•• -,, Comments I CHEMTECH-FORD L/\BOR.\TO RI ES Sample Condltlbn (check If yes) 0 Custody Seals Containers Intact C0C can be matched to bottles Received on Ice Correct Containers(s) Surficent Sample Volume D HcadspJce Present (VOC) Received within Holding Time Plastic Containers A-Pliistic Unpreserved 8-Miscellaneous Plastic C-Cyanide Qt (Na0H) E· Coliform/Ecoli/HPC F-Sulfide Qt (Zn Acetale) l· Mercury 1631 M· Metals Pint (HN03) N-Nutrient Pint (H2S04) R· Radiological (HN03) 5-Sludge Cup</Tubs Q-Plastic Bag Glass Containers D· 625 (Na2S203) G-Glass Unpreserved H· HAAs (NH4CI) J. 508/515/525 (NaZS03) K-515.3 Herbicides 0-Oil & Grease (HCI) P-Phenols (H2S04) T-TOC/T0X (H3P04) U-531 (MCAA, Na2S203) V-524/THMs (Ascorbic Acid) w-s260 voe 11,1 HCII X-Vial Unpreserved V-624/504 (Na2S203) z-Miscellaneous Glass Page 12 of 20 QC Report for Work Order (WO) -22L 1318 Analyte %Rec RPD Limits RPD Max Result Source Cone Blank -EPA 200.8 QC Sample ID: BWL0843-BLK1 Batch: BWL0843 Date Prepared: 12/20/2022 Date Analyzed: 12/20/2022 Units: mg/L Manganese, Dissolved ND Selenium, Dissolved ND Uranium, Dissolved ND LCS -EPA 200.8 QC Sample ID: BWL0843-BSI Batch: BWL0843 Date Prepared: 12/20/2022 Date Analyzed: 12/20/2022 Units: mg/L Manganese, Dissolved 96.7 85 -115 0.039 Selenium, Dissolved 92.6 85 -115 0.037 Uranium, Dissolved 99.1 85 -115 0.040 Matrix Spike -EPA 200.8 QC Sample ID: BWL0843-MS1 Batch: BWL0843 QC Source Sample: 22Ll 318-01 Date Prepared: 12/20/2022 Date Analyzed: 12/20/2022 Units: mg/L Manganese, Dissolved 143 70 -130 0.331 0.273 QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. Selenium, Dissolved Uranium, Dissolved CtF WO#: 22L 1318 www.ChemtechFord.com 94.6 97.1 70 -130 0.051 0.013 70 -130 0.045 0.006 SpkValue MRL DF 0.0100 1.00 0.0050 1.00 0.0003 1.00 0.0400 0.0005 1.00 0.0400 0.0005 1.00 0.0400 0.0003 1.00 0.0400 0.0005 1.00 0.0400 0.0005 1.00 0.0400 0.0003 1.00 Page 13 of20 QC Report for Work Order (WO) -22L 1318 Analyte % Rec RPO Limits RPO Max Result Source Cone Blank -EPA 300.0 QC Sample ID: BWL0787-BLK1 Batch: BWL0787 Date Prepared: 12/19/2022 Date Analyzed: 12/19/2022 Units: mg/L Sulfate ND QC Sample ID: BWL1114-BLKI Batch: BWLI 114 Date Prepared: 12/28/2022 Date Analyzed: 12/28/2022 Units: mg/L Chloride ND LCS -EPA 300.0 QC Sample ID: BWL0787-BS1 Batch: BWL0787 Date Prepared: 12/19/2022 Date Analyzed: 12/19/2022 Units: mg/L Sulfate 89.0 90 -110 44.5 QM-11 -The Laboratory Control Sample recovery was outside acceptance limits. The analytical batch was accepted based on the recovery of the Method Spike. QC Sample ID: BWLI 114-BSI Batch: BWL1114 Date Prepared: 12/28/2022 Date Analyzed: 12/28/2022 Units: mg/L Chloride 98.5 90 -110 49.2 Matrix Spike -EPA 300.0 QC Sample ID: BWL0787-MS1 Batch: BWL0787 QC Source Sample: XXXXXXX-:XX Date Prepared: 12/19/2022 Date Analyzed: 12/19/2022 Units: mg/L Sulfate 109 80 -120 2580 1490 QC Sample ID: BWL0787-MS2 Batch: BWL0787 QC Source Sample: 22L 1318-01 Date Prepared: 12/19/2022 Date Analyzed: 12/19/2022 Units: mg/L Sulfate 97.8 80 -120 1520 1330 QC Sample ID: BWLI 114-MSl Batch: BWLll 14 QC Source Sample: XX:XXXXX-XX Date Prepared: 12/28/2022 Date Analyzed: 12/28/2022 Units: mg/L Chloride 103 80 -120 114 11 .2 QC Sample ID: BWLI l 14-MS2 Batch: BWLI 114 QC Source Sample: XXXXXXX-XX Date Prepared: 12/28/2022 Date Analyzed: 12/29/2022 Units: mg/L Chloride 91.3 80 -120 55.3 45.1 QC Sample ID: BWLl 114-MS3 Batch: BWL1114 QC Source Sample: 22Ll318-0l Date Prepared: 12/28/2022 Date Analyzed: 12/29/2022 Units: mg/L Chloride 100 80 -120 63.4 52.3 Sulfate 80 -120 ND ND QM-4X -The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits. E -The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate (CLP E-flag). Matrix Spike Dup -EPA 300.0 QC Sample ID: BWL0787-MSD1 Batch: BWL0787 QC Source Sample: XXXXXXX-XX Date Prepared: 12/19/2022 Date Analyzed: 12/19/2022 Units: mg/L Sulfate 100 3.27 80 -120 20 2500 1490 QC Sample ID: BWL0787-MSD2 Date Prepared: 12/19/2022 Sulfate QC Sample ID: BWLI 114-MSDI Date Prepared: 12/28/2022 Chloride CtF WO#: 22L 1318 www.ChemtechFord.com Batch: BWL0787 QC Source Sample: 22Ll318-0l Date Analyzed: 12/19/2022 Units: mg/L 91.5 0.838 80 -120 20 1510 1330 Batch: BWLll 14 QC Source Sample: XXXXXXX-XX Date Analyzed: 12/28/2022 Units: mg/L 105 2.16 80 -120 20 116 11 .2 SpkValue MRL OF 1.00 1.00 1.00 1.00 50.0 1.00 1.00 50.0 1.00 1.00 1000 110 1.00 200 22.0 1.00 100 11.0 1.00 11.1 1.11 1.00 11.1 1.11 1.00 11.1 1-11 1.00 1000 110 1.00 200 22.0 1.00 100 11.0 1.00 Page 14 of 20 Analyte QC Sample ID: BWL1114-MSD2 Date Prepared: 12/28/2022 Chloride QC Sample ID: BWLl 114-MSD3 Date Prepared: 12/28/2022 Chloride CtF WO#: 22L 1318 www.ChemtechFord.com QC Report for Work Order (WO) -22L 1318 % Rec RPD Limits RPD Max Result Source Cone Matrix Spike Dup -EPA 300.0 (cont.) Batch: BWLI 114 QC Source Sample: XXXXXXX-XX Date Analyzed: 12/29/2022 Units: mg/L 91.7 0.0945 80 -120 20 55.3 45.1 Batch: BWLll 14 QC Source Sample: 22Ll 318-01 Date Analyzed: 12/29/2022 Units: mg/L 103 0.399 80 -120 20 63.7 52.3 SpkValue MRL DF 11.1 1.11 1.00 11.1 1.11 1.00 Page 15 of 20 QC Report for Work Order (WO) -22L 1318 Analyte % Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -EPA 353.2 QC Sample ID: BWL0741-BLK1 Batch: BWL0741 Date Prepared: 12/16/2022 Date Analyzed: 12/16/2022 Units: mg/L Nitrate+ Nitrite, Total, as N ND 0.100 1.00 QC Sample ID: BWL0742-BLK1 Batch: BWL0742 Date Prepared: 12/16/2022 Date Analyzed: 12/16/2022 Units: mg/L Nitrate + Nitrite, Total, as N ND 0.100 1.00 QC Sample ID: BWLI 157-BLKI Batch: BWL1157 Date Prepared: 12/29/2022 Date Analyzed: 12/29/2022 Units: mg/L Nitrate + Nitrite, Total, as N ND 0.100 1.00 LCS -EPA 353.2 QC Sample ID: BWL0741-BS1 Batch: BWL0741 Date Prepared: 12/16/2022 Date Analyzed: 12/16/2022 Units: mg/L Nitrate + Nitrite, Total, as N 97.8 80 -120 1.96 2.00 0.100 1.00 QC Sample ID: BWL0742-BS 1 Batch: BWL0742 Date Prepared: 12/16/2022 Date Analyzed: 12/16/2022 Units: mg/L Nitrate+ Nitrite, Total, as N 97.9 80 -120 1.96 2.00 0.100 1.00 QC Sample ID: BWLI 157-BSl Batch: BWLI 157 Date Prepared: 12/29/2022 Date Analyzed: 12/29/2022 Units: mg/L Nitrate + Nitrite, Total, as N 94.8 80 -120 1.90 2.00 0.100 1.00 Matrix Spike -EPA 353.2 QC Sample ID: BWL0741-MS1 Batch: BWL0741 QC Source Sample: XXXXXXX-XX Date Prepared: 12/16/2022 Date Analyzed: 12/16/2022 Units: mg/L Nitrate + Nitrite, Total, as N 95.7 80 -120 3.12 2.16 1.00 0.100 1.00 QC Sample ID: BWL0741-MS2 Batch: BWL0741 QC Source Sample: 22Ll 318-01 Date Prepared: 12/16/2022 Date Analyzed: 12/16/2022 Units: mg/L Nitrate + Nitrite, Total, as N 98.5 80 -120 2.28 1.30 1.00 0.100 1.00 QC Sample ID: BWL0742-MS1 Batch: BWL0742 QC Source Sample: 22L1318-06 Date Prepared: 12/16/2022 Date Analyzed: 12/16/2022 Units: mg/L Nitrate+ Nitrite, Total, as N 69.3 80 -120 15.9 15.2 1.00 0.500 5.00 QM-01 0 -The MS recovery was outside acceptance limits but passed Duplicate Spike acceptance limits. The batch was accepted based on the acceptability of the MSD as the batch Spike. QC Sample ID: BWL1157-MS1 Batch: BWL1157 QC Source Sample: XXXXXXX-XX Date Prepared: 12/29/2022 Date Analyzed: 12/29/2022 Units: mg/L Nitrate + Nitrite, Total, as N 96.5 80 -120 0.965 ND 1.00 0.100 1.00 QC Sample ID: BWLl 157-MS2 Batch: BWL1157 QC Source Sample: XX:XXXXX-XX Date Prepared: 12/29/2022 Date Analyzed: 12/29/2022 Units: mg/L Nitrate + Nitrite, Total, as N 108 80 -120 5.98 4.91 1.00 0.500 5.00 Matrix Spike Dup -EPA 353.2 QC Sample ID: BWL0741-MSD1 Batch: BWL0741 QC Source Sample: XXXXXXX-XX Date Prepared: 12/16/2022 Date Analyzed: 12/ I 6/2022 Units: mg/L Nitrate+ Nitrite, Total, as N 98.7 0.958 80 -120 20 3.15 2.16 1.00 0.100 1.00 QC Sample ID: BWL0741-MSD2 Batch: BWL0741 QC Source Sample: 22Ll 318-01 Date Prepared: 12/16/2022 Date Analyzed: 12/16/2022 Units: mg/L Nitrate + Nitrite, Total, as N 114 6.57 80 -120 20 2.44 1.30 1.00 0.100 1.00 QC Sample ID: BWL0742-MSD1 Batch: BWL0742 QC Source Sample: 22Ll 318-06 Date Prepared: 12/16/2022 Date Analyzed: 12/16/2022 Units: mg/L CtF WO#: 22L1318 www.ChemtechFord.com Page 16 of 20 Analyte QC Sample ID: BWL0742-MSD1 Date Prepared: 12/16/2022 Nitrate+ Nitrite, Total, as N QC Sample ID: BWL1157-MSD1 Date Prepared: 12/29/2022 Nitrate + Nitrite, Total, as N QC Sample ID: BWLil57-MSD2 Date Prepared: 12/29/2022 Nitrate + Nitrite, Total, as N CtF WO#: 22L 1318 www.ChemtechFord.com QC Report for Work Order (WO) -22L 1318 %Rec RPD Limits RPD Max Result Source Cone Matrix Spike Dup -EPA 353.2 (cont.) Batch: BWL0742 QC Source Sample: 22Ll 318-06 Date Analyzed: 12/16/2022 Units: mg/L 86.9 1.10 80 -120 20 16.1 15.2 Batch: BWL1157 QC Source Sample: XXXXXXX-XX Date Analyzed: 12/29/2022 Units: mg/L 90.0 6.97 80 -120 20 0.900 ND Batch: BWL1157 QC Source Sample: XXXXXXX-XX Date Analyzed: 12/29/2022 Units: mg/L 98.9 1.50 80 -120 20 5.90 4.91 SpkValue MRL DF 1.00 0.500 5.00 1.00 0.100 1.00 1.00 0.500 5.00 Page 17 of 20 QC Report for Work Order (WO) -22L 1318 Analyte %Rec RPO Limits RPO Max Result Source Cone Blank -EPA 8260D /5030A QC Sample ID: BWL0818-BLK1 Batch: BWL0818 Date Prepared: 12/19/2022 Date Analyzed: 12/19/2022 Units: Chloroform ND LCS -EPA 8260D /5030A QC Sample ID: BWL0818-BS1 Batch: BWL0818 Date Prepared: 12/19/2022 Date Analyzed: 12/19/2022 Units: Chloroform 103 70 -130 10.3 Matrix Spike -EPA 8260D /5030A QC Sample ID: BWL0818-MS1 Batch: BWL0818 QC Source Sample: 2211318-03 Date Prepared: 12/19/2022 Date Analyzed: 12/19/2022 Units: Chloroform 224 70 -130 572 460 MS-High -Estimated high due to Matrix Spike recovery. Matrix Spike Dup -EPA 8260D /5030A QC Sample ID: BWL0818-MSD1 Batch: BWL0818 QC Source Sample: 2211318-03 Date Prepared: 12/19/2022 Date Analyzed: 12/19/2022 Units: Chloroform 166 29.7 70 -130 20 543 460 MS-High -Estimated high due to Matrix Spike recovery. CtF WO#: 22L1318 www.ChemtechFord.com ug/L ug/L ug/L ug/L Spk Value MRL OF 1.0 1.00 10.0 1.0 1.00 50.0 5.0 1.00 50.0 5.0 1.00 Page 18 of 20 Analyte QC Sample ID: BWL0716-BLK1 Date Prepared: 12/16/2022 Total Dissolved Solids (TDS) QC Sample ID: BWL0716-DUP1 Date Prepared: 12/16/2022 Total Dissolved Solids (TDS} QC Sample ID: BWL0716-DUP2 Date Prepared: 12/16/2022 Total Dissolved Solids (TDS) QC Sample ID: BWL0716-BS1 Date Prepared: 12/16/2022 Total Dissolved Solids (TDS) CtF WO#: 22L 1318 www.ChemtechFord.com QC Report for Work Order (WO) -22L 1318 %Rec RPO Limits RPO Max Result Source Cone Spk Value MRL OF Blank -SM 2540 C Batch: BWL0716 Date Analyzed: 12/16/2022 Units: mg/L ND 10 1.00 Duplicate -SM 2540 C Batch: BWL0716 QC Source Sample: 22Ll 318-01 Date Analyzed: 12/16/2022 Units: mg/L 0.8 10 2390 2370 20 1.00 Batch: BWL0716 QC Source Sample: X:XXXXXX-XX Date Analyzed: 12/16/2022 Units: mg/L 2 10 492 480 20 1.00 LCS -SM 2540 C Batch: BWL0716 Date Analyzed: 12/16/2022 Units: mg/L 103 90 -110 412 400 20 1.00 Page 19 of 20 Surrogates Report for Work Order (WO) -22L 1318 QCID Analyte % Rec LCL UCL Result Spk Value Blank -EPA 8260D /5030A BWL0818-BLK1 1,2-Dichloroethane-d4 93.3 64.2 126 9.33 10.0 BWL0818-BLK1 4-Bromofluorobenzene 96.2 71.4 125 9.62 10.0 BWL0818-BLK1 Toluene-dB 100 63.2 129 10.0 10.0 LCS -EPA 8260D /5030A BWL0818-BS1 1,2-Dichloroethane-d4 90.8 64.2 126 9.08 10.0 BWL0818-BS1 4-Bromofluorobenzene 97.8 71.4 125 9.78 10.0 BWL0818-BS1 Toluene-dB 100 63.2 129 10.0 10.0 Matrix Spike -EPA 8260D /5030A BWL0818-MS1 1,2-Dichloroethane-d4 90.9 64.2 126 45.4 50.0 BWL0818-MS1 4-Bromofluorobenzene 98.6 71.4 125 49.3 50.0 BWL0818-MS1 Toluene-dB 100 63.2 129 50.0 50.0 Matrix Spike Dup -EPA 8260D /5030A BWL0818-MSD1 1,2-Dichloroethane-d4 90.3 64.2 126 45.2 50.0 BWL081 B-MSD1 4-Bromofluorobenzene 99.3 71.4 125 49.6 50.0 BWL0818-MSD1 Toluene-dB 100 63.2 129 50.0 50.0 Surrogate Recoveries (Field Samples) LabNumber Analyte Result Spklvl %Rec LCL UCL 8260 Low Level Volatiles 22L1318-03 Toluene-dB 22L131B-03 4-Bromofluorobenzene 22L1318-03 1,2-Dichloroethane-d4 8260 Low Level Volatiles 22L 1318-07 Toluene-dB 22L 1318-07 22L 1318-07 4-Bromofluorobenzene 1,2-Dichloroethane-d4 CtF WO#: 22L1318 www.ChemtechFord.com 10.0 9.71 9.19 10.0 9.60 9.15 10.0 10.0 10.0 10.0 10.0 10.0 100 97.1 91 .9 100 96.0 91 .5 63.2 129 71.4 125 64.2 126 63.2 129 71.4 125 64.2 126 Batch DF BWL0818 1.00 BWL0818 1.00 BWL0818 1.00 BWL0B18 1.00 BWL0818 1.00 BWL0B18 1.00 BWL0B18 1.00 BWL0818 1.00 BWL0818 1.00 BWL0818 1.00 BWL0818 1.00 BWL0818 1.00 Qualifier Page 20 of 20 TabG Quality Assurance and Data Validation Tables G-1 A: Quarterly Field QA/QC Evaluation 1x Casing 2x Casing Location Volume Volume Pumped Volume Volume Check Conductivity RPD pH RPD Temperature RPD Redox RPD Turbidity RPD Dissolved Oxygen MW-01 19.37 39.06 38.74 okay 1780 1776 0.22 6.85 MW-02 12.66 26.04 25.32 okay 3650 3663 0.36 6.97 MW-02 Resample· 12.68 26.04 25.36 okay 3762 3750 0.32 6.85 MW-03a 7.16 14.56 14.32 Pumped Dry 5805 5820 0.26 6.53 MW-05 21.87 45.57 43.74 okay 2849 2843 0.21 7.20 MW-11 29.16 58.59 58.32 okay 3044 3063 0.62 7.05 MW-12 13.68 28.21 27.36 okay 4254 4212 0.99 6.55 MW-14 17.76 36.89 35.52 okay 3703 3716 0.35 6.55 MW-15 20.77 43.4 41.54 okay 4221 4241 0.47 6.74 MW-17 25.85 52.08 51.70 okay 3699 3697 0.05 6.64 MW-18 38.93 78.12 77.86 okay 3398 3395 0.09 6.50 MW-19 53.64 108.50 107.28 okay 1374 1370 0.29 6.53 MW-20 4.97 7.50 9.94 Pumped Dry 5640 5669 0.51 6.91 MW-22 31.05 65.10 62.10 okay 7935 7918 0.21 4.24 MW-23 11.81 24.96 23.62 Pumped Dry 3969 3967 0.05 6.60 MW-24 7.19 15.36 14.38 Pumped Dry 4461 4478 0.38 4.36 MW-24A 7.75 17.28 15.50 Pum_ped Dry 4441 4453 0.27 4.50 MW-25 21.46 43.40 42.92 okay 2769 2730 1.42 6.52 Continuously Pumped MW-26 NA well --3500 NC 6.40 MW-27 23.57 52.08 47.14 okay 1215 1217 0.16 7.13 MW-28 23.10 47.74 46.20 okay 4229 4223 0.14 6.25 MW-29 18.39 39.06 36.78 okay 4574 4577 0.07 6.37 MW-30 22.58 45.57 45.16 okay 2249 2247 0.09 6.80 MW-31 39.48 80.29 78.96 okay 3389 3399 0.29 7.03 MW-32 31 .23 65.10 62.46 okay 3696 3702 0.16 6.22 MW-32 Resample 31.12 65.10 62.24 okay 3717 3720 0.08 6.15 MW-35 8.01 16.27 16.02 okay 4150 4147 0.07 6.50 MW-36 7.30 15.19 14.60 okay 4673 4680 0.15 6.71 MW-37 10.35 15.00 20.70 Pumped Dry 4840 4816 0.50 6.60 MW-38 2.78 5.00 5.56 Pumped Dry 4317 4300 0.39 6.25 MW-39 24.89 52.08 49.78 okay 4797 4798 0.02 3.97 MW-39 Resample 25.00 52.08 50.00 okay 4832 4837 0.10 4.15 MW-40 26.17 53.16 52.34 okay 3895 3900 0.13 6.70 Continuously Pumped TW4-24 NA well -7020 NC 6.46 MW-26 and TW4-24 are continually pumped wells. MW-03a, MW-20, MW-23, MW-24, MW-24A, MW-37, MW-38 were pumped dry and sampled after recovery. NM = Not Measured. The QAP does not require the measurement of redox potential or turbidity in wells that were purged to dryness. RPD = Relative Percent Difference 6.87 0.29 6.97 0.00 6.87 0.29 6.57 0.61 7.23 0.42 7.07 0.28 6.57 0.30 6.56 0.15 6.74 0.00 6.66 0.30 6.51 0.15 6.57 0.61 6.92 0.14 4.24 0.00 6.62 0.30 4.39 0.69 4.52 0.44 6.54 0.31 NC 7,15 0.28 6.26 0.16 6.38 0.16 6.84 0.59 7.01 0.28 6.23 0.16 6.1 7 0.32 6.51 0.15 6.73 0.30 6.60 0.00 6.30 0.80 3.97 0.00 4.13 0.48 6.71 0.15 NC 14.21 14.27 0.42 250 238 4.92 0 0 0.00 14.57 14.50 0.48 424 423 0.24 0 0 0.00 13.86 13.89 0.22 397 395 0.51 0 0 0.00 14.87 14.80 0.47 NM NC NM NC 15.23 15.24 0.07 336 329 2.11 11.3 12.0 6.01 16.00 15.98 0.13 391 389 0.51 0 0 0.00 13.87 14.00 0.93 325 327 0.61 0 0 0.00 15.00 15.00 0.00 363 263 31.95 0 0 0.00 15.09 15.11 0.13 291 291 0.00 0 0 0.00 14.93 14.91 0.13 448 447 0.22 164.0 165.0 0.61 14.73 14.73 0.00 394 391 0.76 0 0 0.00 15.32 14.30 6.89 411 411 0.00 2.7 2.6 3.77 14.13 14.10 0.21 NM NC NM NC 15.34 15.30 0.26 478 479 0.21 4.0 3.9 2.53 14.51 14.45 0.41 NM NC NM NC 15.70 15.73 0.19 NM NC NM NC 14.23 14.25 0.14 NM NC NM NC 15.20 14.10 7.51 407 406 0.25 74.0 76.0 2.67 13.57 NC 397 NC 0 NC 15.18 15.17 0.07 391 389 0.51 8.7 8.4 3.51 15.53 15.50 0.19 397 397 0.00 0 0 0.00 14.68 14.68 0.00 240 238 0.84 7.4 7.5 1.34 14.55 14.51 0.28 334 334 0.00 0 0 0.00 15.39 15.40 0.06 323 321 0.62 378 379 0.26 14.83 14.84 0.07 216 215 0.46 12.0 12.1 0.83 14.67 14.63 0.27 203 202 0.49 39.0 39.0 0.00 14.70 14.65 0.34 306 300 1.98 0 0 0.00 15.12 15.10 0.13 373 371 0.54 0 0 0.00 14.20 14.15 0.35 NM NC NM NC 14.40 14.32 0.56 NM NC NM NC 14.62 14.65 0.20 442 449 1.57 0 0 0.00 14.52 14.52 0.00 392 395 0.76 0 0 0.00 14.90 14.88 0.13 423 422 0.24 2.9 2.9 0.00 15.42 NC 340 NC 0 NC The QAP states that turbidity should be less than 5 Nephelometric Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU are included for information purposes only. 9.1 9.1 18.0 17.9 32.1 32.1 NM 10.4 10.6 9.5 9.6 20.0 19.0 1.9 1.9 18.3 18.3 12.2 12.3 3.1 3.1 133.0 133.0 NM 8.8 8.5 NM NM NM 4.4 4.4 26.3 96.7 96.0 28.3 28.3 6.0 5.8 53.0 53.7 112.0 112.0 4.9 4.9 11.5 11.3 7.4 7.3 75.0 75.0 NM NM 3.4 3.5 5.0 5.0 111.0 111.0 21.0 RPD 0.00 0.56 0.00 NC 1.90 1.05 5.13 0.00 0.00 0.82 0.00 0.00 NC 3.47 NC NC NC 0.00 NC 0.73 0.00 3.39 1.31 0.00 0.00 1.75 1.36 0.00 NC NC 2.90 0.00 0.00 NC G-IB: Accelerated Field QNQC Evaluation 1x Casing 2x Casing Volume Location Volume Volume Pumped Volume Check Conductivity RPD pH MW-11 29.31 59.67 58.62 okay 3083 I 3033 1.64 6.48 I MW-25 21.71 52.08 43.42 okay 3222 I 3218 0.12 6.52 I MW-26 NA Continuously Pumped well --3511 NC 6.38 MW-30 22.90 46.65 45.8 okay 1978 I 1998 1.01 6.35 I MW-31 39.51 80.29 79.02 okay 3486 I 3487 0.03 6.50 I 1x Casing 2x Casing Volume Location Volume Volume Pumped Volume Check Conductivity RPD pH MW-11 29.35 59.67 58.7 okay 3173 I 3167 0.19 7.08 I MW-25 21.61 45.57 43.22 okay 3206 I 3219 0.40 6.54 I MW-26 NA Continuously Pumped well --3524 NC 6.45 MW-30 22.93 47.74 45.86 okay 2245 I 2243 0.09 6.57 I MW-31 39.72 80.29 79.44 okay 3494 I 3491 0.09 6.74 I MW-26 1s a continually pumped well. There are no wells that were pumped dry and sampled after recovery. NM = Not Measured. The OAP does not require the measurement of redox potential or turbidity in wells that were purged to dryness. RPO = Relative Percent Difference November RPD 6.53 0.77 6.55 0.46 NC 6.37 0.31 6.53 0.46 December RPD 7.10 0.28 6.51 0.46 NC 6.59 0.30 6.78 0.59 Dissolved Temperature RPD Redox RPD Turbidity RPD Oxygen 14.62 I 14.70 0.55 483 I 479 0.83 12.0 I 12.3 2.47 6.5 6.3 14.10 I 14.09 0.07 464 I 463 0.22 0 I 0 0.00 1.9 1.8 15.27 NC 461 NC 0 NC 30.7 14.74 I 14.60 0.95 466 I 464 0.43 0 I 0 0.00 51.5 51.0 14.65 I 14.76 0.75 470 I 467 0.64 114.o I 115.o 0.87 112.9 113.0 Dissolved Temperature RPD Redox RPD Turbidity RPD Oxygen 13.84 I 13.83 0.07 364 I 363 0.28 0 I 0 0.00 1.0 1.0 14.25 I 14.28 0.21 410 I 410 0.00 0 I 0 0.00 4.5 4.8 15.70 NC 478 NC 0 NC 34.0 14.27 I 13.27 7.26 449 I 446 0.67 0 I 0 0.00 53.4 53.6 14.21 I 14.24 0.21 427 I 426 0.23 0 I 0 0.00 112.0 111.9 The OAP states that turbidity should be less than 5 Nephelometric Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that has a higher turbidity. The OAP does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU are included for information purposes only. RPD 3.13 5.41 NC 0.98 0.09 RPD 0.00 6.45 NC 0.37 0.09 G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check Trip Blank Acetone 10/10/22 10/19/22 9 14 OK Trip Blank Benzene 10/10/22 10/19/22 9 14 OK Trip Blank Carbon Tetrachloride 10/10/22 10/19/22 9 14 OK Trip Blank Chloroform 10/10/22 10/19/22 9 14 OK Trip Blank Chloromethane 10/10/22 10/19/22 9 14 OK Trip Blank Methyl Ethyl Ketone 10/10/22 10/19/22 9 14 OK Trip Blank Methylene Chloride 10/10/22 10/19/22 9 14 OK Trip Blank Naphthalene 10/10/22 10/19/22 9 14 OK Trip Blank Tetrahydrofuran 10/10/22 10/19/22 9 14 OK Trip Blank Toluene 10/10/22 10/19/22 9 14 OK Trip Blank Xylenes, total 10/10/22 10/19/22 9 14 OK Trip Blank Acetone 10/17/22 10/26/22 9 14 OK Trip Blank Benzene 10/17/22 10/26/22 9 14 OK Trip Blank Carbon Tetrachloride 10/17/22 10/26/22 9 14 OK Trip Blank Chloroform 10/17/22 10/26/22 9 14 OK Trip Blank Chloromethane 10/17/22 10/26/22 9 14 OK Trip Blank Methyl Ethyl Ketone 10/17/22 10/26/22 9 14 OK Trip Blank Methylene Chloride 10/17/22 10/26/22 9 14 OK Trip Blank Naphthalene 10/17/22 10/26/22 9 14 OK Trip Blank Tetrahydrofuran 10/17/22 10/26/22 9 14 OK Trip Blank Toluene 10/17/22 10/26/22 9 14 OK Trip Blank Xylenes, total 10/17/22 10/26/22 9 14 OK Trip Blank Acetone 10/31/22 11/4/22 4 14 OK Trip Blank Benzene 10/31/22 11/4/22 4 14 OK Trip Blank Carbon Tetrachloride 10/31/22 11/4/22 4 14 OK Trip Blank Chloroform 10/31/22 11/4/22 4 14 OK Trip Blank Chloromethane 10/31/22 11/4/22 4 14 OK Trip Blank Methyl Ethyl Ketone 10/31/22 11/4/22 4 14 OK Trip Blank Methylene Chloride 10/31/22 11/4/22 4 14 OK Trip Blank Naphthalene 10/31/22 11/4/22 4 14 OK Trip Blank Tetrahydrofuran 10/31/22 11/4/22 4 14 OK Trip Blank Toluene 10/31/22 11/4/22 4 14 OK Trip Blank Xylenes, total 10/31/22 11/4/22 4 14 OK MW-01 Acetone 10/19/22 10/26/22 7 14 OK MW-01 Arsenic 10/19/22 10/26/22 7 180 OK MW-01 Benzene 10/19/22 10/26/22 7 14 OK MW-01 Beryllium 10/19/22 10/26/22 7 180 OK MW-01 Bicarbonate as CaCO3 10/19/22 10/25/22 6 14 OK MW-01 Cadmium 10/19/22 10/26/22 7 180 OK MW-01 Calcium 10/19/22 10/24/22 5 180 OK MW-01 Carbon Tetrachloride 10/19/22 10/26/22 7 14 OK MW-01 Carbonate as CO3 10/19/22 10/25/22 6 14 OK MW-01 Chloride 10/19/22 11/8/22 20 28 OK MW-01 Chloroform 10/19/22 10/26/22 7 14 OK MW-01 Chloromethane 10/19/22 10/26/22 7 14 OK MW-01 Chromium 10/19/22 10/26/22 7 180 OK MW-01 Cobalt 10/19/22 10/26/22 7 180 OK MW-01 Copper 10/19/22 10/26/22 7 180 OK MW-01 Fluoride 10/19/22 11/2/22 14 28 OK MW-01 Gross Radium Alpha 10/19/22 11/20/22 32 180 OK MW-01 Iron 10/19/22 10/24/22 5 180 OK MW-01 Lead 10/19/22 10/26/22 7 180 OK MW-01 Magnesium 10/19/22 10/24/22 5 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-01 Manganese 10/19/22 10/26/22 7 180 OK MW-01 Mercury 10/19/22 10/26/22 7 180 OK MW-01 Methyl Ethyl Ketone 10/19/22 10/26/22 7 14 OK MW-01 Methylene Chloride 10/19/22 10/26/22 7 14 OK MW-01 Molybdenum 10/19/22 10/26/22 7 180 OK MW-01 Naphthalene 10/19/22 10/26/22 7 14 OK MW-01 Nickel 10/19/22 10/26/22 7 180 OK MW-01 Nitrate + Nitrite as N 10/19/22 10/24/22 5 28 OK MW-01 Nitrogen, Ammonia as N 10/19/22 11/2/22 14 28 OK MW-01 Potassium 10/19/22 10/24/22 5 180 OK MW-01 Selenium 10/19/22 10/26/22 7 180 OK MW-01 Silver 10/19/22 10/26/22 7 180 OK MW-01 Sodium 10/19/22 10/24/22 5 180 OK MW-01 Sulfate 10/19/22 10/25/22 6 28 OK MW-01 Tetrahydrofuran 10/19/22 10/26/22 7 14 OK MW-01 Thallium 10/19/22 10/26/22 7 180 OK MW-01 Tin 10/19/22 10/24/22 5 180 OK MW-01 Toluene 10/19/22 10/26/22 7 14 OK MW-01 Total Dissolved Solids 10/19/22 10/24/22 5 7 OK MW-01 Uranium 10/19/22 10/26/22 7 180 OK MW-01 Vanadium 10/19/22 10/26/22 7 180 OK MW-01 Xylenes, total 10/19/22 10/26/22 7 14 OK MW-01 Zinc 10/19/22 10/26/22 7 180 OK MW-02 Acetone 10/20/22 10/26/22 6 14 OK MW-02 Arsenic 10/20/22 10/26/22 6 180 OK MW-02 Benzene 10/20/22 10/26/22 6 14 OK MW-02 Beryllium 10/20/22 10/26/22 6 180 OK MW-02 Bicarbonate as CaCO3 10/20/22 10/25/22 5 14 OK MW-02 Cadmium 10/20/22 10/26/22 6 180 OK MW-02 Calcium 10/20/22 10/24/22 4 180 OK MW-02 Carbon Tetrachloride 10/20/22 10/26/22 6 14 OK MW-02 Carbonate as CO3 10/20/22 10/25/22 5 14 OK MW-02 Chloride 10/20/22 11/2/22 13 28 OK MW-02 Chloroform 10/20/22 10/26/22 6 14 OK MW-02 Chloromethane 10/20/22 10/26/22 6 14 OK MW-02 Chromium 10/20/22 10/26/22 6 180 OK MW-02 Cobalt 10/20/22 10/26/22 6 180 OK MW-02 Copper 10/20/22 10/26/22 6 180 OK MW-02 Fluoride 10/20/22 11/2/22 13 28 OK MW-02 Iron 10/20/22 10/24/22 4 180 OK MW-02 Lead 10/20/22 10/26/22 6 180 OK MW-02 Magnesium 10/20/22 10/24/22 4 180 OK MW-02 Manganese 10/20/22 10/26/22 6 180 OK MW-02 Mercury 10/20/22 10/26/22 6 180 OK MW-02 Methyl Ethyl Ketone 10/20/22 10/26/22 6 14 OK MW-02 Methylene Chloride 10/20/22 10/26/22 6 14 OK MW-02 Molybdenum 10/20/22 10/26/22 6 180 OK MW-02 Naphthalene 10/20/22 10/26/22 6 14 OK MW-02 Nickel 10/20/22 10/26/22 6 180 OK MW-02 Nitrate+ Nitrite as N 10/20/22 10/25/22 5 28 OK MW-02 Nitrogen, Ammonia as N 10/20/22 11/2/22 13 28 OK MW-02 Potassium 10/20/22 10/24/22 4 180 OK MW-02 Selenium 10/20/22 10/26/22 6 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter N rune Sample Date Analysis Date (Days) Time(Days) Check MW-02 Silver 10/20/22 10/26/22 6 180 OK MW-02 Sodium 10/20/22 10/24/22 4 180 OK MW-02 Sulfate 10/20/22 10/26/22 6 28 OK MW-02 Tetrahydrofuran 10/20/22 10/26/22 6 14 OK MW-02 Thallium 10/20/22 10/26/22 6 180 OK MW-02 Tin 10/20/22 10/24/22 4 180 OK MW-02 Toluene 10/20/22 10/26/22 6 14 OK MW-02 Total Dissolved Solids 10/20/22 10/24/22 4 7 OK MW-02 Uranium 10/20/22 10/26/22 6 180 OK MW-02 Vanadium 10/20/22 10/26/22 6 180 OK MW-02 Xylenes, total 10/20/22 10/26/22 6 14 OK MW-02 Zinc 10/20/22 10/26/22 6 180 OK MW-02 Gross Radium Alpha 11/1/22 11/20/22 19 180 OK MW-03a Acetone 10/19/22 10/26/22 7 14 OK MW-03a Arsenic 10/19/22 10/26/22 7 180 OK MW-03a Benzene 10/19/22 10/26/22 7 14 OK MW-03a Beryllium 10/19/22 10/26/22 7 180 OK MW-03a Bicarbonate as CaCO3 10/19/22 10/25/22 6 14 OK MW-03a Cadmium 10/19/22 10/26/22 7 180 OK MW-03a Calcium 10/19/22 10/24/22 5 180 OK MW-03a Carbon Tetrachloride 10/19/22 10/26/22 7 14 OK MW-03a Carbonate as CO3 10/19/22 10/25/22 6 14 OK MW-03a Chloride 10/19/22 10/25/22 6 28 OK MW-03a Chloroform 10/19/22 10/26/22 7 14 OK MW-03a Chloromethane 10/19/22 10/26/22 7 14 OK MW-03a Chromium 10/19/22 10/26/22 7 180 OK MW-03a Cobalt 10/19/22 10/26/22 7 180 OK MW-03a Coooer 10/19/22 10/26/22 7 180 OK MW-03a Fluoride 10/19/22 11/2/22 14 28 OK MW-03a Gross Radium Alpha 10/19/22 11/20/22 32 180 OK MW-03a Iron 10/19/22 10/24/22 5 180 OK MW-03a Lead 10/19/22 10/26/22 7 180 OK MW-03a Magnesium 10/19/22 10/24/22 5 180 OK MW-03a Manganese 10/19/22 10/26/22 7 180 OK MW-03a Mercury 10/19/22 10/26/22 7 180 OK MW-03a Methyl Ethyl Ketone 10/19/22 10/26/22 7 14 OK MW-03a Methylene Chloride 10/19/22 10/26/22 7 14 OK MW-03a Molybdenum 10/19/22 10/26/22 7 180 OK MW-03a Naphthalene 10/19/22 10/26/22 7 14 OK MW-03a Nickel 10/19/22 10/26/22 7 180 OK MW-03a Nitrate + Nitrite as N 10/19/22 10/24/22 5 28 OK MW-03a Nitrogen, Ammonia as N 10/19/22 11/2/22 14 28 OK MW-03a Potassium 10/19/22 10/24/22 5 180 OK MW-03a Selenium 10/19/22 10/26/22 7 180 OK MW-03a Silver 10/19/22 10/26/22 7 180 OK MW-03a Sodium 10/19/22 10/24/22 5 180 OK MW-03a Sulfate 10/19/22 11/8/22 20 28 OK MW-03a Tetrahydrofuran 10/19/22 10/26/22 7 14 OK MW-03a Thallium 10/19/22 10/26/22 7 180 OK MW-03a Tin 10/19/22 10/24/22 5 180 OK MW-03a Toluene 10/19/22 10/26/22 7 14 OK MW-03a Total Dissolved Solids 10/19/22 10/24/22 5 7 OK MW-03a Uranium 10/19/22 10/26/22 7 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-03a Vanadium 10/19/22 10/26/22 7 180 OK MW-03a Xylenes, total 10/19/22 10/26/22 7 14 OK MW-03a Zinc 10/19/22 10/26/22 7 180 OK MW-05 Acetone 10/12/22 10/19/22 7 14 OK MW-05 Arsenic 10/12/22 10/21/22 9 180 OK MW-05 Benzene 10/12/22 10/19/22 7 14 OK MW-05 Beryllium 10/12/22 10/21/22 9 180 OK MW-05 Bicarbonate as CaCO3 10/12/22 10/19/22 7 14 OK MW-05 Cadmium 10/12/22 10/21/22 9 180 OK MW-05 Calcium 10/12/22 10/24/22 12 180 OK MW-05 Carbon Tetrachloride 10/12/22 10/19/22 7 14 OK MW-05 Carbonate as CO3 10/12/22 10/19/22 7 14 OK MW-05 Chloride 10/12/22 10/17/22 5 28 OK MW-05 Chloroform 10/12/22 10/19/22 7 14 OK MW-05 Chloromethane 10/12/22 10/19/22 7 14 OK MW-05 Chromium 10/12/22 10/21/22 9 180 OK MW-05 Cobalt 10/12/22 10/21/22 9 180 OK MW-05 Copper 10/12/22 10/21/22 9 180 OK MW-05 Fluoride 10/12/22 10/17/22 5 28 OK MW-05 Gross Radium Alpha 10/12/22 11/14/22 33 180 OK MW-05 Iron 10/12/22 10/24/22 12 180 OK MW-05 Lead 10/12/22 10/21/22 9 180 OK MW-05 Magnesium 10/12/22 10/24/22 12 180 OK MW-05 Manganese 10/12/22 10/21/22 9 180 OK MW-05 Mercury 10/12/22 10/18/22 6 180 OK MW-05 Methyl Ethyl Ketone 10/12/22 10/19/22 7 14 OK MW-05 Methylene Chloride 10/12/22 10/19/22 7 14 OK MW-05 Molybdenum 10/12/22 10/21/22 9 180 OK MW-05 Naphthalene 10/12/22 10/19/22 7 14 OK MW-05 Nickel 10/12/22 10/21/22 9 180 OK MW-05 Nitrate + Nitrite as N 10/12/22 10/18/22 6 28 OK MW-05 Nitrogen, Ammonia as N 10/12/22 10/27/22 15 28 OK MW-05 Potassium 10/12/22 10/24/22 12 180 OK MW-05 Selenium 10/12/22 10/21/22 9 180 OK MW-05 Silver 10/12/22 10/21/22 9 180 OK MW-05 Sodium 10/12/22 10/24/22 12 180 OK MW-05 Sulfate 10/12/22 10/28/22 16 28 OK MW-05 Tetrahydrofuran 10/12/22 10/19/22 7 14 OK MW-05 Thallium 10/12/22 10/21/22 9 180 OK MW-05 Tin 10/12/22 10/24/22 12 180 OK MW-05 Toluene 10/12/22 10/19/22 7 14 OK MW-05 Total Dissolved Solids 10/12/22 10/17/22 5 7 OK MW-05 Uranium 10/12/22 10/21/22 9 180 OK MW-05 Vanadium 10/12/22 10/21/22 9 180 OK MW-05 Xylenes, total 10/12/22 10/19/22 7 14 OK MW-05 Zinc 10/12/22 10/21/22 9 180 OK MW-11 Acetone 10/10/22 10/19/22 9 14 OK MW-11 Arsenic 10/10/22 10/21/22 11 180 OK MW-11 Benzene 10/10/22 10/19/22 9 14 OK MW-11 Beryllium 10/10/22 10/21/22 11 180 OK MW-11 Bicarbonate as CaCO3 10/10/22 10/19/22 9 14 OK MW-11 Cadmium 10/10/22 10/21/22 11 180 OK MW-11 Calcium 10/10/22 10/24/22 14 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-11 Carbon Tetrachloride 10/10/22 10/19/22 9 14 OK MW-11 Carbonate as CO3 10/10/22 10/19/22 9 14 OK MW-11 Chloride 10/10/22 10/17/22 7 28 OK MW-11 Chloroform 10/10/22 10/19/22 9 14 OK MW-11 Chloromethane 10/10/22 10/19/22 9 14 OK MW-11 Chromium 10/10/22 10/21/22 11 180 OK MW-11 Cobalt 10/10/22 10/21/22 11 180 OK MW-11 Coooer 10/10/22 10/21/22 11 180 OK MW-11 Fluoride 10/10/22 10/17/22 7 28 OK MW-11 Gross Radium Alpha 10/10/22 11/14/22 35 180 OK MW-11 Iron 10/10/22 10/24/22 14 180 OK MW-11 Lead 10/10/22 10/21/22 11 180 OK MW-11 Magnesium 10/10/22 10/24/22 14 180 OK MW-11 Manganese 10/10/22 10/21/22 11 180 OK MW-11 Mercury 10/10/22 10/18/22 8 180 OK MW-11 Methyl Ethyl Ketone 10/10/22 10/19/22 9 14 OK MW-11 Methylene Chloride 10/10/22 10/19/22 9 14 OK MW-11 Molybdenum 10/10/22 10/21/22 11 180 OK MW-11 Naphthalene 10/10/22 10/19/22 9 14 OK MW-11 Nickel 10/10/22 10/21/22 11 180 OK MW-11 Nitrate+ Nitrite as N 10/10/22 10/18/22 8 28 OK MW-11 Nitrogen, Ammonia as N 10/10/22 10/27/22 17 28 OK MW-11 Potassium 10/10/22 10/24/22 14 180 OK MW-11 Selenium 10/10/22 10/21/22 11 180 OK MW-11 Silver 10/10/22 10/21/22 11 180 OK MW-11 Sodium 10/10/22 10/24/22 14 180 OK MW-11 Sulfate 10/10/22 10/19/22 9 28 OK MW-11 Tetrahydrofuran 10/10/22 10/19/22 9 14 OK MW-11 Thallium 10/10/22 10/21/22 11 180 OK MW-11 Tin 10/10/22 10/24/22 14 180 OK MW-11 Toluene 10/10/22 10/19/22 9 14 OK MW-11 Total Dissolved Solids 10/10/22 10/17/22 7 7 OK MW-11 Uranium 10/10/22 10/21/22 11 180 OK MW-11 Vanadium 10/10/22 10/21/22 11 180 OK MW-11 Xvlenes, total 10/10/22 10/19/22 9 14 OK MW-11 Zinc 10/10/22 10/21/22 11 180 OK MW-12 Acetone 10/13/22 10/19/22 6 14 OK MW-12 Arsenic 10/13/22 10/21/22 8 180 OK MW-12 Benzene 10/13/22 10/19/22 6 14 OK MW-12 Beryllium 10/13/22 10/21/22 8 180 OK MW-12 Bicarbonate as CaCO3 10/13/22 10/19/22 6 14 OK MW-12 Cadmium 10/13/22 10/21/22 8 180 OK MW-12 Calcium 10/13/22 10/24/22 11 180 OK MW-12 Carbon Tetrachloride 10/13/22 10/19/22 6 14 OK MW-12 Carbonate as CO3 10/13/22 10/19/22 6 14 OK MW-12 Chloride 10/13/22 10/17/22 4 28 OK MW-12 Chloroform 10/13/22 10/19/22 6 14 OK MW-12 Chloromethane 10/13/22 10/19/22 6 14 OK MW-12 Chromium 10/13/22 10/21/22 8 180 OK MW-12 Cobalt 10/13/22 10/21/22 8 180 OK MW-12 Coooer 10/13/22 10/21/22 8 180 OK MW-12 Fluoride 10/13/22 10/17/22 4 28 OK MW-12 Gross Radium Alpha 10/13/22 11/14/22 32 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-12 Iron 10/13/22 10/24/22 11 180 OK MW-12 Lead 10/13/22 10/21/22 8 180 OK MW-12 Magnesium 10/13/22 10/24/22 11 180 OK MW-12 Manganese 10/13/22 10/21/22 8 180 OK MW-12 Mercury 10/13/22 10/18/22 5 180 OK MW-12 Methyl Ethyl Ketone 10/13/22 10/19/22 6 14 OK MW-12 Methylene Chloride 10/13/22 10/19/22 6 14 OK MW-12 Molybdenum 10/13/22 10/21/22 8 180 OK MW-12 Naphthalene 10/13/22 10/19/22 6 14 OK MW-12 Nickel 10/13/22 10/21/22 8 180 OK MW-12 Nitrate + Nitrite as N 10/13/22 10/18/22 5 28 OK MW-12 Nitrogen, Ammonia as N 10/13/22 10/27/22 14 28 OK MW-12 Potassium 10/13/22 10/24/22 11 180 OK MW-12 Selenium 10/13/22 10/21/22 8 180 OK MW-12 Silver 10/13/22 10/21/22 8 180 OK MW-12 Sodium 10/13/22 10/24/22 11 180 OK MW-12 Sulfate 10/13/22 10/20/22 7 28 OK MW-12 Tetrahydrofuran 10/13/22 10/19/22 6 14 OK MW-12 Thallium 10/13/22 10/21/22 8 180 OK MW-12 Tin 10/13/22 10/24/22 II 180 OK MW-12 Toluene 10/13/22 10/19/22 6 14 OK MW-12 Total Dissolved Solids 10/13/22 10/17/22 4 7 OK MW-12 Uranium 10/13/22 10/21/22 8 180 OK MW-12 Vanadium 10/13/22 10/21/22 8 180 OK MW-12 Xylenes, total 10/13/22 10/19/22 6 14 OK MW-12 Zinc 10/13/22 10/21/22 8 180 OK MW-14 Acetone 10/11/22 10/19/22 8 14 OK MW-14 Arsenic 10/11/22 10/21/22 IO 180 OK MW-14 Benzene 10/11/22 10/19/22 8 14 OK MW-14 Beryllium 10/11/22 10/21/22 10 180 OK MW-14 Bicarbonate as CaCO3 10/11/22 10/19/22 8 14 OK MW-14 Cadmium 10/11/22 10/21/22 10 180 OK MW-14 Calcium 10/11/22 10/24/22 13 180 OK MW-14 Carbon Tetrachloride 10/11/22 10/19/22 8 14 OK MW-14 Carbonate as CO3 10/11/22 10/19/22 8 14 OK MW-14 Chloride 10/11/22 10/17/22 6 28 OK MW-14 Chloroform 10/11/22 10/19/22 8 14 OK MW-14 Chloromethane 10/11/22 10/19/22 8 14 OK MW-14 Chromium 10/11/22 10/21/22 10 180 OK MW-14 Cobalt 10/11/22 10/21/22 10 180 OK MW-14 Coooer 10/11/22 10/21/22 10 180 OK MW-14 Fluoride 10/11/22 10/17/22 6 28 OK MW-14 Gross Radium Alpha 10/11/22 11/14/22 34 180 OK MW-14 Iron 10/11/22 10/24/22 13 180 OK MW-14 Lead 10/11/22 10/21/22 IO 180 OK MW-14 Magnesium 10/11/22 10/24/22 13 180 OK MW-14 Manganese 10/11/22 10/21/22 IO 180 OK MW-14 Mercury 10/11/22 10/18/22 7 180 OK MW-14 Methyl Ethyl Ketone 10/11/22 10/19/22 8 14 OK MW-14 Methylene Chloride 10/11/22 10/19/22 8 14 OK MW-14 Molybdenum 10/11/22 10/21/22 IO 180 OK MW-14 Naphthalene 10/11/22 10/19/22 8 14 OK MW-14 Nickel 10/11/22 10/21/22 10 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-14 Nitrate + Nitrite as N 10/11/22 10/18/22 7 28 OK MW-14 Nitrogen, Ammonia as N 10/11/22 10/27/22 16 28 OK MW-14 Potassium 10/11/22 10/24/22 13 180 OK MW-14 Selenium 10/11/22 10/21/22 10 180 OK MW-14 Silver 10/11/22 10/21/22 10 180 OK MW-14 Sodium 10/11/22 10/24/22 13 180 OK MW-14 Sulfate 10/11/22 10/19/22 8 28 OK MW-14 Tetrahydrofuran 10/11/22 10/19/22 8 14 OK MW-14 Thallium 10/11/22 10/21/22 10 180 OK MW-14 Tin 10/11/22 10/24/22 13 180 OK MW-14 Toluene 10/11/22 10/19/22 8 14 OK MW-14 Total Dissolved Solids 10/11/22 10/17/22 6 7 OK MW-14 Uranium 10/11/22 10/21/22 10 180 OK MW-14 Vanadium 10/11/22 10/21/22 10 180 OK MW-14 Xylenes, total 10/11/22 10/19/22 8 14 OK MW-14 Zinc 10/11/22 10/21/22 10 180 OK MW-15 Acetone 10/12/22 10/19/22 7 14 OK MW-15 Arsenic 10/12/22 10/21/22 9 180 OK MW-15 Benzene 10/12/22 10/19/22 7 14 OK MW-15 Beryllium 10/12/22 10/21/22 9 180 OK MW-15 Bicarbonate as CaCO3 10/12/22 10/19/22 7 14 OK MW-15 Cadmium 10/12/22 10/21/22 9 180 OK MW-15 Calcium 10/12/22 10/24/22 12 180 OK MW-15 Carbon Tetrachloride 10/12/22 10/19/22 7 14 OK MW-15 Carbonate as CO3 10/12/22 10/19/22 7 14 OK MW-15 Chloride 10/12/22 10/17/22 5 28 OK MW-15 Chloroform 10/12/22 10/19/22 7 14 OK MW-15 Chloromethane 10/12/22 10/19/22 7 14 OK MW-15 Chromium 10/12/22 10/21/22 9 180 OK MW-15 Cobalt 10/12/22 10/21/22 9 180 OK MW-15 Copper 10/12/22 10/21/22 9 180 OK MW-15 Fluoride 10/12/22 10/17/22 5 28 OK MW-15 Gross Radium Alpha 10/12/22 11/14/22 33 180 OK MW-15 Iron 10/12/22 10/24/22 12 180 OK MW-15 Lead 10/12/22 10/21/22 9 180 OK MW-15 Magnesium 10/12/22 10/24/22 12 180 OK MW-15 Manganese 10/12/22 10/21/22 9 180 OK MW-15 Mercury 10/12/22 10/18/22 6 180 OK MW-15 Methyl Ethyl Ketone 10/12/22 10/19/22 7 14 OK MW-15 Methylene Chloride 10/12/22 10/19/22 7 14 OK MW-15 Molybdenum 10/12/22 10/21/22 9 180 OK MW-15 Naphthalene 10/12/22 10/19/22 7 14 OK MW-15 Nickel 10/12/22 10/21/22 9 180 OK MW-15 Nitrate + Nitrite as N 10/12/22 10/18/22 6 28 OK MW-15 Nitrogen, Ammonia as N 10/12/22 10/27/22 15 28 OK MW-15 Potassium 10/12/22 10/24/22 12 180 OK MW-15 Selenium 10/12/22 10/21/22 9 180 OK MW-15 Silver 10/12/22 10/21/22 9 180 OK MW-15 Sodium 10/12/22 10/24/22 12 180 OK MW-15 Sulfate 10/12/22 10/20/22 8 28 OK MW-15 Tetrahydrofuran 10/12/22 10/19/22 7 14 OK MW-15 Thallium 10/12/22 10/21/22 9 180 OK MW-15 Tin 10/12/22 10/24/22 12 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-15 Toluene 10/12/22 10/19/22 7 14 OK MW-15 Total Dissolved Solids 10/12/22 10/17/22 5 7 OK MW-15 Uranium 10/12/22 10/21/22 9 180 OK MW-15 Vanadium 10/12/22 10/21/22 9 180 OK MW-15 Xylenes, total 10/12/22 10/19/22 7 14 OK MW-15 Zinc 10/12/22 10/21/22 9 180 OK MW-17 Acetone 10/17/22 10/26/22 9 14 OK MW-17 Arsenic 10/17/22 10/26/22 9 180 OK MW-17 Benzene 10/17/22 10/26/22 9 14 OK MW-17 Beryllium 10/17/22 10/26/22 9 180 OK MW-17 Bicarbonate as CaCO3 10/17/22 10/25/22 8 14 OK MW-17 Cadmium 10/17/22 10/26/22 9 180 OK MW-17 Calcium 10/17/22 10/24/22 7 180 OK MW-17 Carbon Tetrachloride 10/17/22 10/26/22 9 14 OK MW-17 Carbonate as CO3 10/17/22 10/25/22 8 14 OK MW-17 Chloride 10/17/22 10/25/22 8 28 OK MW-17 Chloroform 10/17/22 10/26/22 9 14 OK MW-17 Chloromethane 10/17/22 10/26/22 9 14 OK MW-17 Chromium 10/17/22 10/26/22 9 180 OK MW-17 Cobalt 10/17/22 10/26/22 9 180 OK MW-17 Copper 10/17/22 10/26/22 9 180 OK MW-17 Fluoride 10/17/22 11/2/22 16 28 OK MW-17 Gross Radium Alpha 10/17/22 11/20/22 34 180 OK MW-17 Iron 10/17/22 10/24/22 7 180 OK MW-17 Lead 10/17/22 10/26/22 9 180 OK MW-17 Magnesium 10/17/22 10/24/22 7 180 OK MW-17 Manganese 10/17/22 10/26/22 9 180 OK MW-17 Mercury 10/17/22 10/26/22 9 180 OK MW-17 Methyl Ethyl Ketone 10/17/22 10/26/22 9 14 OK MW-17 Methylene Chloride 10/17/22 10/26/22 9 14 OK MW-17 Molybdenum 10/17/22 10/26/22 9 180 OK MW-17 Naphthalene 10/17/22 10/26/22 9 14 OK MW-17 Nickel 10/17/22 10/26/22 9 180 OK MW-17 Nitrate + Nitrite as N 10/17/22 10/24/22 7 28 OK MW-17 Nitrogen, Ammonia as N 10/17/22 11/2/22 16 28 OK MW-17 Potassium 10/17/22 10/24/22 7 180 OK MW-17 Selenium 10/17/22 10/26/22 9 180 OK MW-17 Silver 10/17/22 10/26/22 9 180 OK MW-17 Sodium 10/17/22 10/24/22 7 180 OK MW-17 Sulfate 10/17/22 10/25/22 8 28 OK MW-17 Tetrahydrofuran 10/17/22 10/26/22 9 14 OK MW-17 Thallium 10/17/22 10/26/22 9 180 OK MW-17 Tin 10/17/22 10/24/22 7 180 OK MW-17 Toluene 10/17/22 10/26/22 9 14 OK MW-17 Total Dissolved Solids 10/17/22 10/24/22 7 7 OK MW-17 Uranium 10/17/22 10/26/22 9 180 OK MW-17 Vanadium 10/17/22 10/26/22 9 180 OK MW-17 Xylenes, total 10/17/22 10/26/22 9 14 OK MW-17 Zinc 10/17/22 10/26/22 9 180 OK MW-18 Acetone 10/18/22 10/26/22 8 14 OK MW-18 Arsenic 10/18/22 10/26/22 8 180 OK MW-18 Benzene 10/18/22 10/26/22 8 14 OK MW-18 Beryllium 10/18/22 10/26/22 8 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-18 Bicarbonate as CaCO3 10/18/22 10/25/22 7 14 OK MW-18 Cadmium 10/18/22 10/26/22 8 180 OK MW-18 Calcium 10/18/22 10/24/22 6 180 OK MW-18 Carbon Tetrachloride 10/18/22 10/26/22 8 14 OK MW-18 Carbonate as CO3 10/18/22 10/25/22 7 14 OK MW-18 Chloride 10/18/22 10/25/22 7 28 OK MW-18 Chloroform 10/18/22 10/26/22 8 14 OK MW-18 Chloromethane 10/18/22 10/26/22 8 14 OK MW-18 Chromium 10/18/22 10/26/22 8 180 OK MW-18 Cobalt 10/18/22 10/26/22 8 180 OK MW-18 Copper 10/18/22 10/26/22 8 180 OK MW-18 Fluoride 10/18/22 11/2/22 15 28 OK MW-18 Gross Radium Alpha 10/18/22 11/20/22 33 180 OK MW-18 Iron 10/18/22 10/24/22 6 180 OK MW-18 Lead 10/18/22 10/26/22 8 180 OK MW-18 Magnesium 10/18/22 10/24/22 6 180 OK MW-18 Manganese 10/18/22 10/26/22 8 180 OK MW-18 Mercury 10/18/22 10/26/22 8 180 OK MW-18 Methyl Ethyl Ketone 10/18/22 10/26/22 8 14 OK MW-18 Methylene Chloride 10/18/22 10/26/22 8 14 OK MW-18 Molybdenum 10/18/22 10/26/22 8 180 OK MW-18 Naphthalene 10/18/22 10/26/22 8 14 OK MW-18 Nickel 10/18/22 10/26/22 8 180 OK MW-18 Nitrate + Nitrite as N 10/18/22 10/24/22 6 28 OK MW-18 Nitrogen, Ammonia as N 10/18/22 11/2/22 15 28 OK MW-18 Potassium 10/18/22 10/24/22 6 180 OK MW-18 Selenium 10/18/22 10/26/22 8 180 OK MW-18 Silver 10/18/22 10/26/22 8 180 OK MW-18 Sodium 10/18/22 10/24/22 6 180 OK MW-18 Sulfate 10/18/22 11/8/22 21 28 OK MW-18 Tetrahydrofuran 10/18/22 10/26/22 8 14 OK MW-18 Thallium 10/18/22 10/26/22 8 180 OK MW-18 Tin 10/18/22 10/24/22 6 180 OK MW-18 Toluene 10/18/22 10/26/22 8 14 OK MW-18 Total Dissolved Solids 10/18/22 10/24/22 6 7 OK MW-18 Uranium 10/18/22 10/26/22 8 180 OK MW-18 Vanadium 10/18/22 10/26/22 8 180 OK MW-18 Xylenes, total 10/18/22 10/26/22 8 14 OK MW-18 Zinc 10/18/22 10/26/22 8 180 OK MW-19 Acetone 10/17/22 10/26/22 9 14 OK MW-19 Arsenic 10/17/22 10/26/22 9 180 OK MW-19 Benzene 10/17/22 10/26/22 9 14 OK MW-19 Beryllium 10/17/22 10/26/22 9 180 OK MW-19 Bicarbonate as CaCO3 10/17/22 10/25/22 8 14 OK MW-19 Cadmium 10/17/22 10/26/22 9 180 OK MW-19 Calcium 10/17/22 10/24/22 7 180 OK MW-19 Carbon Tetrachloride 10/17/22 10/26/22 9 14 OK MW-19 Carbonate as CO3 10/17/22 10/25/22 8 14 OK MW-19 Chloride 10/17/22 10/25/22 8 28 OK MW-19 Chloroform 10/17/22 10/26/22 9 14 OK MW-19 Chloromethane 10/17/22 10/26/22 9 14 OK MW-19 Chromium 10/17/22 10/26/22 9 180 OK MW-19 Cobalt 10/17/22 10/26/22 9 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-19 Copper 10/17/22 10/26/22 9 180 OK MW-19 Fluoride 10/17/22 11/2/22 16 28 OK MW-19 Gross Radium Alpha 10/17/22 11/20/22 34 180 OK MW-19 Iron 10/17/22 10/24/22 7 180 OK MW-19 Lead 10/17/22 10/26/22 9 180 OK MW-19 Magnesium 10/17/22 10/24/22 7 180 OK MW-19 Manganese 10/17/22 10/26/22 9 180 OK MW-19 Mercury 10/17/22 10/26/22 9 180 OK MW-19 Methyl Ethyl Ketone 10/17/22 10/26/22 9 14 OK MW-19 Methylene Chloride 10/17/22 10/26/22 9 14 OK MW-19 Molybdenum 10/17/22 10/26/22 9 180 OK MW-19 Naphthalene 10/17/22 10/26/22 9 14 OK MW-19 Nickel 10/17/22 10/26/22 9 180 OK MW-19 Nitrate + Nitrite as N 10/17/22 10/24/22 7 28 OK MW-19 Nitrogen, Ammonia as N 10/17/22 11/2/22 16 28 OK MW-19 Potassium 10/17/22 10/24/22 7 180 OK MW-19 Selenium 10/17/22 10/26/22 9 180 OK MW-19 Silver 10/17/22 10/26/22 9 180 OK MW-19 Sodium 10/17/22 10/24/22 7 180 OK MW-19 Sulfate 10/17/22 10/25/22 8 28 OK MW-19 Tetrahydrofuran 10/17/22 10/26/22 9 14 OK MW-19 Thallium 10/17/22 10/26/22 9 180 OK MW-19 Tin 10/17/22 10/24/22 7 180 OK MW-19 Toluene 10/17/22 10/26/22 9 14 OK MW-19 Total Dissolved Solids 10/17/22 10/24/22 7 7 OK MW-19 Uranium 10/17/22 10/26/22 9 180 OK MW-19 Vanadium 10/17/22 10/26/22 9 180 OK MW-19 Xylenes, total 10/17/22 10/26/22 9 14 OK MW-19 Zinc 10/17/22 10/26/22 9 180 OK MW-20 Acetone 11/1/22 11/4/22 3 14 OK MW-20 Arsenic 11/1/22 11/14/22 13 180 OK MW-20 Benzene 11/1/22 11/4/22 3 14 OK MW-20 Beryllium 11/1/22 11/14/22 13 180 OK MW-20 Bicarbonate as CaCO3 11/1/22 11/3/22 2 14 OK MW-20 Cadmium 11/1/22 11/14/22 13 180 OK MW-20 Calcium 11/1/22 11/8/22 7 180 OK MW-20 Carbon Tetrachloride 11/1/22 11/4/22 3 14 OK MW-20 Carbonate as CO3 11/1/22 11/3/22 2 14 OK MW-20 Chloride 11/1/22 11/14/22 13 28 OK MW-20 Chloroform 11/1/22 11/4/22 3 14 OK MW-20 Chloromethane 11/1/22 11/4/22 3 14 OK MW-20 Chromium 11/1/22 11/14/22 13 180 OK MW-20 Cobalt 11/1/22 11/14/22 13 180 OK MW-20 Copper 11/1/22 11/14/22 13 180 OK MW-20 Fluoride 11/1/22 11/14/22 13 28 OK MW-20 Gross Radium Alpha 11/1/22 11/20/22 19 180 OK MW-20 Iron 11/1/22 11/8/22 7 180 OK MW-20 Lead 11/1/22 11/14/22 13 180 OK MW-20 Magnesium 11/1/22 11/8/22 7 180 OK MW-20 Manganese 11/1/22 11/14/22 13 180 OK MW-20 Mercury 11/1/22 11/10/22 9 180 OK MW-20 Methyl Ethyl Ketone 11/1/22 11/4/22 3 14 OK MW-20 Methylene Chloride 11/1/22 11/4/22 3 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-20 Molybdenum 11/1/22 11/14/22 13 180 OK MW-20 Naphthalene 11/1/22 11/4/22 3 14 OK MW-20 Nickel 11/1/22 11/14/22 13 180 OK MW-20 Nitrate + Nitrite as N 11/1/22 11/8/22 7 28 OK MW-20 Nitrogen, Ammonia as N 11/1/22 11/14/22 13 28 OK MW-20 Potassium 11/1/22 11/8/22 7 180 OK MW-20 Selenium 11/1/22 11/14/22 13 180 OK MW-20 Silver 11/1/22 11/14/22 13 180 OK MW-20 Sodium 11/1/22 11/8/22 7 180 OK MW-20 Sulfate 11/1/22 11/19/22 18 28 OK MW-20 Tetrahydrofuran 11/1/22 11/4/22 3 14 OK MW-20 Thallium 11/1/22 11/14/22 13 180 OK MW-20 Tin 11/1/22 11/8/22 7 180 OK MW-20 Toluene 11/1/22 11/4/22 3 14 OK MW-20 Total Dissolved Solids 11/1/22 11/4/22 3 7 OK MW-20 Uranium 11/1/22 11/14/22 13 180 OK MW-20 Vanadium 11/1/22 11/14/22 13 180 OK MW-20 Xylenes, total 11/1/22 11/4/22 3 14 OK MW-20 Zinc 11/1/22 11/14/22 13 180 OK MW-22 Acetone 10/19/22 10/26/22 7 14 OK MW-22 Arsenic 10/19/22 10/26/22 7 180 OK MW-22 Benzene 10/19/22 10/26/22 7 14 OK MW-22 Beryllium 10/19/22 10/26/22 7 180 OK MW-22 Bicarbonate as CaCO3 10/19/22 10/25/22 6 14 OK MW-22 Cadmium 10/19/22 10/26/22 7 180 OK MW-22 Calcium 10/19/22 11/8/22 20 180 OK MW-22 Carbon Tetrachloride 10/19/22 10/26/22 7 14 OK MW-22 Carbonate as CO3 10/19/22 10/25/22 6 14 OK MW-22 Chloride 10/19/22 10/25/22 6 28 OK MW-22 Chloroform 10/19/22 10/26/22 7 14 OK MW-22 Chloromethane 10/19/22 10/26/22 7 14 OK MW-22 Chromium 10/19/22 10/26/22 7 180 OK MW-22 Cobalt 10/19/22 10/26/22 7 180 OK MW-22 Copper 10/19/22 10/26/22 7 180 OK MW-22 Fluoride 10/19/22 11/2/22 14 28 OK MW-22 Gross Radium Alpha 10/19/22 11/20/22 32 180 OK MW-22 Iron 10/19/22 10/24/22 5 180 OK MW-22 Lead 10/19/22 10/26/22 7 180 OK MW-22 Magnesium 10/19/22 11/8/22 20 180 OK MW-22 Manganese 10/19/22 10/26/22 7 180 OK MW-22 Mercury 10/19/22 10/26/22 7 180 OK MW-22 Methyl Ethyl Ketone 10/19/22 10/26/22 7 14 OK MW-22 Methylene Chloride 10/19/22 10/26/22 7 14 OK MW-22 Molybdenum 10/19/22 10/26/22 7 180 OK MW-22 Naphthalene 10/19/22 10/26/22 7 14 OK MW-22 Nickel 10/19/22 10/26/22 7 180 OK MW-22 Nitrate + Nitrite as N 10/19/22 10/24/22 5 28 OK MW-22 Nitrogen, Ammonia as N 10/19/22 11/2/22 14 28 OK MW-22 Potassium 10/19/22 11/8/22 20 180 OK MW-22 Selenium 10/19/22 10/26/22 7 180 OK MW-22 Silver 10/19/22 10/26/22 7 180 OK MW-22 Sodium 10/19/22 11/8/22 20 180 OK MW-22 Sulfate 10/19/22 10/26/22 7 28 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-22 Tetrahydrofuran 10/19/22 10/26/22 7 14 OK MW-22 Thallium 10/19/22 10/26/22 7 180 OK MW-22 Tin 10/19/22 10/24/22 5 180 OK MW-22 Toluene 10/19/22 10/26/22 7 14 OK MW-22 Total Dissolved Solids 10/19/22 10/24/22 5 7 OK MW-22 Uranium 10/19/22 10/26/22 7 180 OK MW-22 Vanadium 10/19/22 10/26/22 7 180 OK MW-22 Xylenes, total 10/19/22 10/26/22 7 14 OK MW-22 Zinc 10/19/22 10/26/22 7 180 OK MW-23 Acetone 11/1/22 11/4/22 3 14 OK MW-23 Arsenic 11/1/22 11/14/22 13 180 OK MW-23 Benzene 11/1/22 11/4/22 3 14 OK MW-23 Beryllium 11/1/22 11/14/22 13 180 OK MW-23 Bicarbonate as CaCO3 11/1/22 11/3/22 2 14 OK MW-23 Cadmium 11/1/22 11/14/22 13 180 OK MW-23 Calcium 11/1/22 11/8/22 7 180 OK MW-23 Carbon Tetrachloride 11/1/22 11/4/22 3 14 OK MW-23 Carbonate as CO3 11/1/22 11/3/22 2 14 OK MW-23 Chloride 11/1/22 11/14/22 13 28 OK MW-23 Chloroform 11/1/22 11/4/22 3 14 OK MW-23 Chloromethane 11/1/22 11/4/22 3 14 OK MW-23 Chromium 11/1/22 11/14/22 13 180 OK MW-23 Cobalt 11/1/22 11/14/22 13 180 OK MW-23 Cooner 11/1/22 11/14/22 13 180 OK MW-23 Fluoride 11/1/22 11/14/22 13 28 OK MW-23 Gross Radium Alpha 11/1/22 11/20/22 19 180 OK MW-23 Iron 11/1/22 11/8/22 7 180 OK MW-23 Lead 11/1/22 11/14/22 13 180 OK MW-23 Magnesium 11/1/22 11/8/22 7 180 OK MW-23 Manganese 11/1/22 11/14/22 13 180 OK MW-23 Mercury 11/1/22 11/10/22 9 180 OK MW-23 Methyl Ethyl Ketone 11/1/22 11/4/22 3 14 OK MW-23 Methylene Chloride 11/1/22 11/4/22 3 14 OK MW-23 Molybdenum 11/1/22 11/14/22 13 180 OK MW-23 Naphthalene 11/1/22 11/4/22 3 14 OK MW-23 Nickel 11/1/22 11/14/22 13 180 OK MW-23 Nitrate + Nitrite as N 11/1/22 11/8/22 7 28 OK MW-23 Nitrogen, Ammonia as N 11/1/22 11/14/22 13 28 OK MW-23 Potassium 11/1/22 11/8/22 7 180 OK MW-23 Selenium 11/1/22 11/14/22 13 180 OK MW-23 Silver 11/1/22 11/14/22 13 180 OK MW-23 Sodium 11/1/22 11/8/22 7 180 OK MW-23 Sulfate 11/1/22 11/14/22 13 28 OK MW-23 Tetrahydrofuran 11/1/22 11/4/22 3 14 OK MW-23 Thallium 11/1/22 11/14/22 13 180 OK MW-23 Tin 11/1/22 11/8/22 7 180 OK MW-23 Toluene 11/1/22 11/4/22 3 14 OK MW-23 Total Dissolved Solids 11/1/22 11/4/22 3 7 OK MW-23 Uranium 11/1/22 11/14/22 13 180 OK MW-23 Vanadium 11/1/22 11/14/22 13 180 OK MW-23 Xylenes, total 11/1/22 11/4/22 3 14 OK MW-23 Zinc 11/1/22 11/14/22 13 180 OK MW-24 Acetone 11/2/22 11/4/22 2 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Davs) Time (Days) Check MW-24 Arsenic 11/2/22 11/14/22 12 180 OK MW-24 Benzene 11/2/22 11/4/22 2 14 OK MW-24 Beryllium 11/2/22 11/14/22 12 180 OK MW-24 Bicarbonate as CaCO3 11/2/22 11/4/22 2 14 OK MW-24 Cadmium 11/2/22 11/14/22 12 180 OK MW-24 Calcium 11/2/22 11/8/22 6 180 OK MW-24 Carbon Tetrachloride 11/2/22 11/4/22 2 14 OK MW-24 Carbonate as CO3 11/2/22 11/4/22 2 14 OK MW-24 Chloride 11/2/22 11/14/22 12 28 OK MW-24 Chloroform 11/2/22 11/4/22 2 14 OK MW-24 Chloromethane 11/2/22 11/4/22 2 14 OK MW-24 Chromium 11/2/22 11/14/22 12 180 OK MW-24 Cobalt 11/2/22 11/14/22 12 180 OK MW-24 Coooer 11/2/22 11/14/22 12 180 OK MW-24 Fluoride 11/2/22 11/14/22 12 28 OK MW-24 Gross Radium Alpha 11/2/22 11/20/22 18 180 OK MW-24 Iron 11/2/22 11/8/22 6 180 OK MW-24 Lead 11/2/22 11/14/22 12 180 OK MW-24 Magnesium 11/2/22 11/8/22 6 180 OK MW-24 Manganese 11/2/22 11/14/22 12 180 OK MW-24 Mercury 11/2/22 11/10/22 8 180 OK MW-24 Methyl Ethyl Ketone 11/2/22 11/4/22 2 14 OK MW-24 Methylene Chloride 11/2/22 11/4/22 2 14 OK MW-24 Molybdenum 11/2/22 11/14/22 12 180 OK MW-24 Naphthalene 11/2/22 11/4/22 2 14 OK MW-24 Nickel 11/2/22 11/14/22 12 180 OK MW-24 Nitrate + Nitrite as N 11/2/22 11/8/22 6 28 OK MW-24 Nitrogen, Ammonia as N 11/2/22 11/14/22 12 28 OK MW-24 Potassium 11/2/22 11/8/22 6 180 OK MW-24 Selenium 11/2/22 11/14/22 12 180 OK MW-24 Silver 11/2/22 11/14/22 12 180 OK MW-24 Sodium 11/2/22 11/8/22 6 180 OK MW-24 Sulfate 11/2/22 11/14/22 12 28 OK MW-24 Tetrahydrofuran 11/2/22 11/4/22 2 14 OK MW-24 Thallium 11/2/22 11/14/22 12 180 OK MW-24 Tin 11/2/22 11/8/22 6 180 OK MW-24 Toluene 11/2/22 11/4/22 2 14 OK MW-24 Total Dissolved Solids 11/2/22 11/4/22 2 7 OK MW-24 Uranium 11/2/22 11/14/22 12 180 OK MW-24 Vanadium 11/2/22 11/14/22 12 180 OK MW-24 Xylenes, total 11/2/22 11/4/22 2 14 OK MW-24 Zinc 11/2/22 11/14/22 12 180 OK MW-24A Acetone 11/2/22 11/4/22 2 14 OK MW-24A Arsenic 11/2/22 11/14/22 12 180 OK MW-24A Benzene 11/2/22 11/4/22 2 14 OK MW-24A Beryllium 11/2/22 11/14/22 12 180 OK MW-24A Bicarbonate as CaCO3 11/2/22 11/4/22 2 14 OK MW-24A Cadmium 11/2/22 11/14/22 12 180 OK MW-24A Calcium 11/2/22 11/8/22 6 180 OK MW-24A Carbon Tetrachloride 11/2/22 11/4/22 2 14 OK MW-24A Carbonate as CO3 11/2/22 11/4/22 2 14 OK MW-24A Chloride 11/2/22 11/14/22 12 28 OK MW-24A Chloroform 11/2/22 11/4/22 2 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-24A Chloromethane 11/2/22 11/4/22 2 14 OK MW-24A Chromium 11/2/22 11/14/22 12 180 OK MW-24A Cobalt 11/2/22 11/14/22 12 180 OK MW-24A Copper 11/2/22 11/14/22 12 180 OK MW-24A Fluoride 11/2/22 11/14/22 12 28 OK MW-24A Gross Radium Alpha 11/2/22 11/20/22 18 180 OK MW-24A Iron 11/2/22 11/8/22 6 180 OK MW-24A Lead 11/2/22 11/14/22 12 180 OK MW-24A Magnesium 11/2/22 11/8/22 6 180 OK MW-24A Manganese 11/2/22 11/14/22 12 180 OK MW-24A Mercury 11/2/22 11/10/22 8 180 OK MW-24A Methyl Ethyl Ketone 11/2/22 11/4/22 2 14 OK MW-24A Methylene Chloride 11/2/22 11/4/22 2 14 OK MW-24A Molybdenum 11/2/22 11/14/22 12 180 OK MW-24A Naphthalene 11/2/22 11/4/22 2 14 OK MW-24A Nickel 11/2/22 11/14/22 12 180 OK MW-24A Nitrate+ Nitrite as N 11/2/22 11/8/22 6 28 OK MW-24A Nitrogen, Ammonia as N 11/2/22 11/14/22 12 28 OK MW-24A Potassium 11/2/22 11/8/22 6 180 OK MW-24A Selenium 11/2/22 11/14/22 12 180 OK MW-24A Silver 11/2/22 11/14/22 12 180 OK MW-24A Sodium 11/2/22 11/8/22 6 180 OK MW-24A Sulfate 11/2/22 11/14/22 12 28 OK MW-24A Tetrahydrofuran 11/2/22 11/4/22 2 14 OK MW-24A Thallium 11/2/22 11/14/22 12 180 OK MW-24A Tin 11/2/22 11/8/22 6 180 OK MW-24A Toluene 11/2/22 11/4/22 2 14 OK MW-24A Total Dissolved Solids 11/2/22 11/4/22 2 7 OK MW-24A Uranium 11/2/22 11/14/22 12 180 OK MW-24A Vanadium 11/2/22 11/14/22 12 180 OK MW-24A Xylenes, total 11/2/22 11/4/22 2 14 OK MW-24A Zinc 11/2/22 11/14/22 12 180 OK MW-25 Acetone 10/10/22 10/19/22 9 14 OK MW-25 Arsenic 10/10/22 10/21/22 11 180 OK MW-25 Benzene 10/10/22 10/19/22 9 14 OK MW-25 Beryllium 10/10/22 10/21/22 11 180 OK MW-25 Bicarbonate as CaCO3 10/10/22 10/19/22 9 14 OK MW-25 Cadmium 10/10/22 10/21/22 11 180 OK MW-25 Calcium 10/10/22 10/24/22 14 180 OK MW-25 Carbon Tetrachloride 10/10/22 10/19/22 9 14 OK MW-25 Carbonate as CO3 10/10/22 10/19/22 9 14 OK MW-25 Chloride 10/10/22 10/17/22 7 28 OK MW-25 Chloroform 10/10/22 10/19/22 9 14 OK MW-25 Chloromethane 10/10/22 10/19/22 9 14 OK MW-25 Chromium 10/10/22 10/21/22 11 180 OK MW-25 Cobalt 10/10/22 10/21/22 11 180 OK MW-25 Copper 10/10/22 10/21/22 11 180 OK MW-25 Fluoride 10/10/22 10/17/22 7 28 OK MW-25 Gross Radium Alpha 10/10/22 11/14/22 35 180 OK MW-25 Iron 10/10/22 10/24/22 14 180 OK MW-25 Lead 10/10/22 10/21/22 11 180 OK MW-25 Magnesium 10/10/22 10/24/22 14 180 OK MW-25 Manganese 10/10/22 10/21/22 11 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-25 Mercury 10/10/22 10/18/22 8 180 OK MW-25 Methyl Ethyl Ketone 10/10/22 10/19/22 9 14 OK MW-25 Methylene Chloride 10/10/22 10/19/22 9 14 OK MW-25 Molybdenum 10/10/22 10/21/22 11 180 OK MW-25 Naphthalene 10/10/22 10/19/22 9 14 OK MW-25 Nickel 10/10/22 10/21/22 11 180 OK MW-25 Nitrate + Nitrite as N 10/10/22 10/18/22 8 28 OK MW-25 Nitrogen, Ammonia as N 10/10/22 10/27/22 17 28 OK MW-25 Potassium 10/10/22 10/24/22 14 180 OK MW-25 Selenium 10/10/22 10/21/22 11 180 OK MW-25 Silver 10/10/22 10/21/22 11 180 OK MW-25 Sodium 10/10/22 10/24/22 14 180 OK MW-25 Sulfate 10/10/22 10/19/22 9 28 OK MW-25 Tetrahydrofuran 10/10/22 10/19/22 9 14 OK MW-25 Thallium 10/10/22 10/21/22 11 180 OK MW-25 Tin 10/10/22 10/24/22 14 180 OK MW-25 Toluene 10/10/22 10/19/22 9 14 OK MW-25 Total Dissolved Solids 10/10/22 10/17/22 7 7 OK MW-25 Uranium 10/10/22 10/21/22 11 180 OK MW-25 Vanadium 10/10/22 10/21/22 11 180 OK MW-25 Xylenes, total 10/10/22 10/19/22 9 14 OK MW-25 Zinc 10/10/22 10/21/22 11 180 OK MW-26 Acetone 10/13/22 10/19/22 6 14 OK MW-26 Arsenic 10/13/22 10/21/22 8 180 OK MW-26 Benzene 10/13/22 10/19/22 6 14 OK MW-26 Beryllium 10/13/22 10/21/22 8 180 OK MW-26 Bicarbonate as CaCO3 10/13/22 10/19/22 6 14 OK MW-26 Cadmium 10/13/22 10/21/22 8 180 OK MW-26 Calcium 10/13/22 10/24/22 11 180 OK MW-26 Carbon Tetrachloride 10/13/22 10/19/22 6 14 OK MW-26 Carbonate as CO3 10/13/22 10/19/22 6 14 OK MW-26 Chloride 10/13/22 10/18/22 5 28 OK MW-26 Chloroform 10/13/22 10/19/22 6 14 OK MW-26 Chloromethane 10/13/22 10/19/22 6 14 OK MW-26 Chromium 10/13/22 10/21/22 8 180 OK MW-26 Cobalt 10/13/22 10/21/22 8 180 OK MW-26 Coooer 10/13/22 10/21/22 8 180 OK MW-26 Fluoride 10/13/22 10/18/22 5 28 OK MW-26 Gross Radium Alpha 10/13/22 11/14/22 32 180 OK MW-26 Iron 10/13/22 10/24/22 11 180 OK MW-26 Lead 10/13/22 10/21/22 8 180 OK MW-26 Magnesium 10/13/22 10/24/22 11 180 OK MW-26 Manganese 10/13/22 10/21/22 8 180 OK MW-26 Mercury 10/13/22 10/18/22 5 180 OK MW-26 Methyl Ethyl Ketone 10/13/22 10/19/22 6 14 OK MW-26 Methylene Chloride 10/13/22 10/19/22 6 14 OK MW-26 Molybdenum 10/13/22 10/21/22 8 180 OK MW-26 Naphthalene 10/13/22 10/19/22 6 14 OK MW-26 Nickel 10/13/22 10/21/22 8 180 OK MW-26 Nitrate + Nitrite as N 10/13/22 10/18/22 5 28 OK MW-26 Nitrogen, Ammonia as N 10/13/22 10/27/22 14 28 OK MW-26 Potassium 10/13/22 10/24/22 11 180 OK MW-26 Selenium 10/13/22 10/21/22 8 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-26 Silver 10/13/22 10/21/22 8 180 OK MW-26 Sodium 10/13/22 10/24/22 11 180 OK MW-26 Sulfate 10/13/22 10/20/22 7 28 OK MW-26 Tetrahydrofuran 10/13/22 10/19/22 6 14 OK MW-26 Thallium 10/13/22 10/21/22 8 180 OK MW-26 Tin 10/13/22 10/24/22 11 180 OK MW-26 Toluene 10/13/22 10/19/22 6 14 OK MW-26 Total Dissolved Solids 10/13/22 10/17/22 4 7 OK MW-26 Uranium 10/13/22 10/21/22 8 180 OK MW-26 Vanadium 10/13/22 10/21/22 8 180 OK MW-26 Xylenes, total 10/13/22 10/19/22 6 14 OK MW-26 Zinc 10/13/22 10/21/22 8 180 OK MW-27 Acetone 10/19/22 10/26/22 7 14 OK MW-27 Arsenic 10/19/22 10/26/22 7 180 OK MW-27 Benzene 10/19/22 10/26/22 7 14 OK MW-27 Beryllium 10/19/22 10/26/22 7 180 OK MW-27 Bicarbonate as CaCO3 10/19/22 10/25/22 6 14 OK MW-27 Cadmium 10/19/22 10/26/22 7 180 OK MW-27 Calcium 10/19/22 10/24/22 5 180 OK MW-27 Carbon Tetrachloride 10/19/22 10/26/22 7 14 OK MW-27 Carbonate as CO3 10/19/22 10/25/22 6 14 OK MW-27 Chloride 10/19/22 10/25/22 6 28 OK MW-27 Chloroform 10/19/22 10/26/22 7 14 OK MW-27 Chloromethane 10/19/22 10/26/22 7 14 OK MW-27 Chromium 10/19/22 10/26/22 7 180 OK MW-27 Cobalt 10/19/22 10/26/22 7 180 OK MW-27 Copper 10/19/22 10/26/22 7 180 OK MW-27 Fluoride 10/19/22 11/2/22 14 28 OK MW-27 Gross Radium Alpha 10/19/22 11/20/22 32 180 OK MW-27 Iron 10/19/22 10/24/22 5 180 OK MW-27 Lead 10/19/22 10/26/22 7 180 OK MW-27 Magnesium 10/19/22 10/24/22 5 180 OK MW-27 Manganese 10/19/22 10/26/22 7 180 OK MW-27 Mercury 10/19/22 10/26/22 7 180 OK MW-27 Methyl Ethyl Ketone 10/19/22 10/26/22 7 14 OK MW-27 Methylene Chloride 10/19/22 10/26/22 7 14 OK MW-27 Molybdenum 10/19/22 10/26/22 7 180 OK MW-27 Naphthalene 10/19/22 10/26/22 7 14 OK MW-27 Nickel 10/19/22 10/26/22 7 180 OK MW-27 Nitrate + Nitrite as N 10/19/22 10/25/22 6 28 OK MW-27 Nitrogen, Ammonia as N 10/19/22 11/2/22 14 28 OK MW-27 Potassium 10/19/22 10/24/22 5 180 OK MW-27 Selenium 10/19/22 10/26/22 7 180 OK MW-27 Silver 10/19/22 10/26/22 7 180 OK MW-27 Sodium 10/19/22 10/24/22 5 180 OK MW-27 Sulfate 10/19/22 10/25/22 6 28 OK MW-27 Tetrahydrofuran 10/19/22 10/26/22 7 14 OK MW-27 Thallium 10/19/22 10/26/22 7 180 OK MW-27 Tin 10/19/22 10/24/22 5 180 OK MW-27 Toluene 10/19/22 10/26/22 7 14 OK MW-27 Total Dissolved Solids 10/19/22 10/24/22 5 7 OK MW-27 Uranium 10/19/22 10/26/22 7 180 OK MW-27 Vanadium 10/19/22 10/26/22 7 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-27 Xylenes, total 10/19/22 10/26/22 7 14 OK MW-27 Zinc 10/19/22 10/26/22 7 180 OK MW-28 Acetone 10/12/22 10/19/22 7 14 OK MW-28 Arsenic 10/12/22 10/21/22 9 180 OK MW-28 Benzene 10/12/22 10/19/22 7 14 OK MW-28 Beryllium 10/12/22 10/21/22 9 180 OK MW-28 Bicarbonate as CaCO3 10/12/22 10/19/22 7 14 OK MW-28 Cadmium 10/12/22 10/21/22 9 180 OK MW-28 Calcium 10/12/22 10/24/22 12 180 OK MW-28 Carbon Tetrachloride 10/12/22 10/19/22 7 14 OK MW-28 Carbonate as CO3 10/12/22 10/19/22 7 14 OK MW-28 Chloride 10/12/22 10/20/22 8 28 OK MW-28 Chloroform 10/12/22 10/19/22 7 14 OK MW-28 Chloromethane 10/12/22 10/19/22 7 14 OK MW-28 Chromium 10/12/22 10/21/22 9 180 OK MW-28 Cobalt 10/12/22 10/21/22 9 180 OK MW-28 Coooer 10/12/22 10/21/22 9 180 OK MW-28 Fluoride 10/12/22 10/17/22 5 28 OK MW-28 Gross Radium Alpha 10/12/22 11/14/22 33 180 OK MW-28 Iron 10/12/22 10/24/22 12 180 OK MW-28 Lead 10/12/22 10/21/22 9 180 OK MW-28 Magnesium 10/12/22 10/24/22 12 180 OK MW-28 Manganese 10/12/22 10/21/22 9 180 OK MW-28 Mercury 10/12/22 10/18/22 6 180 OK MW-28 Methyl Ethyl Ketone 10/12/22 10/19/22 7 14 OK MW-28 Methylene Chloride 10/12/22 10/19/22 7 14 OK MW-28 Molybdenum 10/12/22 10/21/22 9 180 OK MW-28 Naphthalene 10/12/22 10/19/22 7 14 OK MW-28 Nickel 10/12/22 10/21/22 9 180 OK MW-28 Nitrate + Nitrite as N 10/12/22 10/18/22 6 28 OK MW-28 Nitrogen, Ammonia as N 10/12/22 10/27/22 15 28 OK MW-28 Potassium 10/12/22 10/24/22 12 180 OK MW-28 Selenium 10/12/22 10/21/22 9 180 OK MW-28 Silver 10/12/22 10/21/22 9 180 OK MW-28 Sodium 10/12/22 10/24/22 12 180 OK MW-28 Sulfate 10/12/22 10/28/22 16 28 OK MW-28 Tetrahydrofuran 10/12/22 10/19/22 7 14 OK MW-28 Thallium 10/12/22 10/21/22 9 180 OK MW-28 Tin 10/12/22 10/24/22 12 180 OK MW-28 Toluene 10/12/22 10/19/22 7 14 OK MW-28 Total Dissolved Solids 10/12/22 10/17/22 5 7 OK MW-28 Uranium 10/12/22 10/21/22 9 180 OK MW-28 Vanadium 10/12/22 10/21/22 9 180 OK MW-28 Xylenes, total 10/12/22 10/19/22 7 14 OK MW-28 Zinc 10/12/22 10/21/22 9 180 OK MW-29 Acetone 10/12/22 10/19/22 7 14 OK MW-29 Arsenic 10/12/22 10/21/22 9 180 OK MW-29 Benzene 10/12/22 10/19/22 7 14 OK MW-29 Beryllium 10/12/22 10/21/22 9 180 OK MW-29 Bicarbonate as CaCO3 10/12/22 10/19/22 7 14 OK MW-29 Cadmium 10/12/22 10/21/22 9 180 OK MW-29 Calcium 10/12/22 10/24/22 12 180 OK MW-29 Carbon Tetrachloride 10/12/22 10/19/22 7 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-29 Carbonate as CO3 10/12/22 10/19/22 7 14 OK MW-29 Chloride 10/12/22 10/17/22 5 28 OK MW-29 Chloroform 10/12/22 10/19/22 7 14 OK MW-29 Chloromethane 10/12/22 10/19/22 7 14 OK MW-29 Chromium 10/12/22 10/21/22 9 180 OK MW-29 Cobalt 10/12/22 10/21/22 9 180 OK MW-29 Copper 10/12/22 10/21/22 9 180 OK MW-29 Fluoride 10/12/22 10/17/22 5 28 OK MW-29 Gross Radium Alpha 10/12/22 11/14/22 33 180 OK MW-29 Iron 10/12/22 10/24/22 12 180 OK MW-29 Lead 10/12/22 10/21/22 9 180 OK MW-29 Magnesium 10/12/22 10/24/22 12 180 OK MW-29 Manganese 10/12/22 10/21/22 9 180 OK MW-29 Mercury 10/12/22 10/18/22 6 180 OK MW-29 Methyl Ethyl Ketone 10/12/22 10/19/22 7 14 OK MW-29 Methylene Chloride 10/12/22 10/19/22 7 14 OK MW-29 Molybdenum 10/12/22 10/21/22 9 180 OK MW-29 Naphthalene 10/12/22 10/19/22 7 14 OK MW-29 Nickel 10/12/22 10/21/22 9 180 OK MW-29 Nitrate + Nitrite as N 10/12/22 10/18/22 6 28 OK MW-29 Nitrogen, Ammonia as N 10/12/22 10/27/22 15 28 OK MW-29 Potassium 10/12/22 10/24/22 12 180 OK MW-29 Selenium 10/12/22 10/21/22 9 180 OK MW-29 Silver 10/12/22 10/21/22 9 180 OK MW-29 Sodium 10/12/22 10/24/22 12 180 OK MW-29 Sulfate 10/12/22 10/20/22 8 28 OK MW-29 Tetiahydrofuran 10/12/22 10/19/22 7 14 OK MW-29 Thallium 10/12/22 10/21/22 9 180 OK MW-29 Tin 10/12/22 10/24/22 12 180 OK MW-29 Toluene 10/12/22 10/19/22 7 14 OK MW-29 Total Dissolved Solids 10/12/22 10/17/22 5 7 OK MW-29 Uranium 10/12/22 10/21/22 9 180 OK MW-29 Vanadium 10/12/22 10/21/22 9 180 OK MW-29 Xylenes, total 10/12/22 10/19/22 7 14 OK MW-29 Zinc 10/12/22 10/21/22 9 180 OK MW-30 Acetone 10/13/22 10/19/22 6 14 OK MW-30 Arsenic 10/13/22 10/21/22 8 180 OK MW-30 Benzene 10/13/22 10/19/22 6 14 OK MW-30 Beryllium 10/13/22 10/21/22 8 180 OK MW-30 Bicarbonate as CaCO3 10/13/22 10/19/22 6 14 OK MW-30 Cadmium 10/13/22 10/21/22 8 180 OK MW-30 Calcium 10/13/22 10/24/22 11 180 OK MW-30 Carbon Tetrachloride 10/13/22 10/19/22 6 14 OK MW-30 Carbonate as CO3 10/13/22 10/19/22 6 14 OK MW-30 Chloride 10/13/22 10/20/22 7 28 OK MW-30 Chloroform 10/13/22 10/19/22 6 14 OK MW-30 Chloromethane 10/13/22 10/19/22 6 14 OK MW-30 Chromium 10/13/22 10/21/22 8 180 OK MW-30 Cobalt 10/13/22 10/21/22 8 180 OK MW-30 Cooner 10/13/22 10/21/22 8 180 OK MW-30 Fluoride 10/13/22 10/17/22 4 28 OK MW-30 Gross Radium Alpha 10/13/22 11/14/22 32 180 OK MW-30 Iron 10/13/22 10/24/22 11 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-30 Lead 10/13/22 10/21/22 8 180 OK MW-30 Magnesium 10/13/22 10/24/22 11 180 OK MW-30 Manganese 10/13/22 10/21/22 8 180 OK MW-30 Mercury 10/13/22 10/18/22 5 180 OK MW-30 Methyl Ethyl Ketone 10/13/22 10/19/22 6 14 OK MW-30 Methylene Chloride 10/13/22 10/19/22 6 14 OK MW-30 Molybdenum 10/13/22 10/21/22 8 180 OK MW-30 Naphthalene 10/13/22 10/19/22 6 14 OK MW-30 Nickel 10/13/22 10/21/22 8 180 OK MW-30 Nitrate + Nitrite as N 10/13/22 10/18/22 5 28 OK MW-30 Nitrogen, Ammonia as N 10/13/22 10/27/22 14 28 OK MW-30 Potassium 10/13/22 10/24/22 11 180 OK MW-30 Selenium 10/13/22 10/21/22 8 180 OK MW-30 Silver 10/13/22 10/21/22 8 180 OK MW-30 Sodium 10/13/22 10/24/22 11 180 OK MW-30 Sulfate 10/13/22 10/20/22 7 28 OK MW-30 Tetrahydrofuran 10/13/22 10/19/22 6 14 OK MW-30 Thallium 10/13/22 10/21/22 8 180 OK MW-30 Tin 10/13/22 10/24/22 11 180 OK MW-30 Toluene 10/13/22 10/19/22 6 14 OK MW-30 Total Dissolved Solids 10/13/22 10/18/22 5 7 OK MW-30 Uranium 10/13/22 10/21/22 8 180 OK MW-30 Vanadium 10/13/22 10/21/22 8 180 OK MW-30 Xylenes, total 10/13/22 10/19/22 6 14 OK MW-30 Zinc 10/13/22 10/21/22 8 180 OK MW-31 Acetone 10/11/22 10/19/22 8 14 OK MW-31 Arsenic 10/11/22 10/21/22 10 180 OK MW-31 Benzene 10/11/22 10/19/22 8 14 OK MW-31 Beryllium 10/11/22 10/21/22 10 180 OK MW-31 Bicarbonate as CaCO3 10/11/22 10/19/22 8 14 OK MW-31 Cadmium 10/11/22 10/21/22 10 180 OK MW-31 Calcium 10/11/22 10/24/22 13 180 OK MW-31 Carbon Tetrachloride 10/11/22 10/19/22 8 14 OK MW-31 Carbonate as CO3 10/11/22 10/19/22 8 14 OK MW-31 Chloride 10/11/22 10/19/22 8 28 OK MW-31 Chloroform 10/11/22 10/19/22 8 14 OK MW-31 Chloromethane 10/11/22 10/19/22 8 14 OK MW-31 Chromium 10/11/22 10/21/22 10 180 OK MW-31 Cobalt 10/11/22 10/21/22 10 180 OK MW-31 Coooer 10/11/22 10/21/22 10 180 OK MW-31 Fluoride 10/11/22 10/17/22 6 28 OK MW-31 Gross Radium Alpha 10/11/22 11/14/22 34 180 OK MW-31 Iron 10/11/22 10/24/22 13 180 OK MW-31 Lead 10/11/22 10/21/22 10 180 OK MW-31 Magnesium 10/11/22 10/24/22 13 180 OK MW-31 Manganese 10/11/22 10/21/22 10 180 OK MW-31 Mercury 10/11/22 10/18/22 7 180 OK MW-31 Methyl Ethyl Ketone 10/11/22 10/19/22 8 14 OK MW-31 Methylene Chloride 10/11/22 10/19/22 8 14 OK MW-31 Molybdenum 10/11/22 10/21/22 10 180 OK MW-31 Naphthalene 10/11/22 10/19/22 8 14 OK MW-31 Nickel 10/11/22 10/21/22 10 180 OK MW-31 Nitrate + Nitrite as N 10/11/22 10/18/22 7 28 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-31 Nitrogen, Ammonia as N 10/11/22 10/27/22 16 28 OK MW-31 Potassium 10/11/22 10/24/22 13 180 OK MW-31 Selenium 10/11/22 10/21/22 10 180 OK MW-31 Silver 10/11/22 10/21/22 10 180 OK MW-31 Sodium 10/11/22 10/24/22 13 180 OK MW-31 Sulfate 10/11/22 10/19/22 8 28 OK MW-31 Tetrahydrofuran 10/11/22 10/19/22 8 14 OK MW-31 Thallium 10/11/22 10/21/22 10 180 OK MW-31 Tin 10/11/22 10/24/22 13 180 OK MW-31 Toluene 10/11/22 10/19/22 8 14 OK MW-31 Total Dissolved Solids 10/11/22 10/17/22 6 7 OK MW-31 Uranium 10/11/22 10/21/22 10 180 OK MW-31 Vanadium 10/11/22 10/21/22 10 180 OK MW-31 Xylenes, total 10/11/22 10/19/22 8 14 OK MW-31 Zinc 10/11/22 10/21/22 10 180 OK MW-32 Acetone 10/11/22 10/19/22 8 14 OK MW-32 Arsenic 10/11/22 10/21/22 10 180 OK MW-32 Benzene 10/11/22 10/19/22 8 14 OK MW-32 Beryllium 10/11/22 10/21/22 10 180 OK MW-32 Bicarbonate as CaCO3 10/11/22 10/19/22 8 14 OK MW-32 Cadmium 10/11/22 10/21/22 IO 180 OK MW-32 Calcium 10/11/22 10/24/22 13 180 OK MW-32 Carbon Tetrachloride 10/11/22 10/19/22 8 14 OK MW-32 Carbonate as CO3 10/11/22 10/19/22 8 14 OK MW-32 Chloride 10/11/22 10/17/22 6 28 OK MW-32 Chloroform 10/11/22 10/19/22 8 14 OK MW-32 Chloromethane 10/11/22 10/19/22 8 14 OK MW-32 Chromium 10/11/22 10/21/22 10 180 OK MW-32 Cobalt 10/11/22 10/21/22 10 180 OK MW-32 Copper 10/11/22 10/21/22 10 180 OK MW-32 Fluoride 10/11/22 10/17/22 6 28 OK MW-32 Iron 10/11/22 10/24/22 13 180 OK MW-32 Lead 10/11/22 10/21/22 10 180 OK MW-32 Magnesium 10/11/22 10/24/22 13 180 OK MW-32 Manganese 10/11/22 10/21/22 10 180 OK MW-32 Mercury 10/11/22 10/18/22 7 180 OK MW-32 Methyl Ethyl Ketone 10/11/22 10/19/22 8 14 OK MW-32 Methylene Chloride 10/11/22 10/19/22 8 14 OK MW-32 Molybdenum 10/11/22 10/21/22 10 180 OK MW-32 Naphthalene 10/11/22 10/19/22 8 14 OK MW-32 Nickel 10/11/22 10/21/22 10 180 OK MW-32 Nitrate + Nitrite as N 10/11/22 10/18/22 7 28 OK MW-32 Nitrogen, Ammonia as N 10/11/22 10/27/22 16 28 OK MW-32 Potassium 10/11/22 10/24/22 13 180 OK MW-32 Selenium 10/11/22 10/21/22 10 180 OK MW-32 Silver 10/11/22 10/21/22 10 180 OK MW-32 Sodium 10/11/22 10/24/22 13 180 OK MW-32 Sulfate 10/11/22 10/19/22 8 28 OK MW-32 Tetrahydrofuran 10/11/22 10/19/22 8 14 OK MW-32 Thallium 10/11/22 10/21/22 10 180 OK MW-32 Tin 10/11/22 10/24/22 13 180 OK MW-32 Toluene 10/11/22 10/19/22 8 14 OK MW-32 Total Dissolved Solids 10/11/22 10/17/22 6 7 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-32 Uranium 10/11/22 10/21/22 10 180 OK MW-32 Vanadium 10/11/22 10/21/22 10 180 OK MW-32 Xylenes, total 10/11/22 10/19/22 8 14 OK MW-32 Zinc 10/11/22 10/21/22 10 180 OK MW-32 Gross Radium Alpha 10/31/22 11/20/22 20 180 OK MW-35 Acetone 10/31/22 11/4/22 4 14 OK MW-35 Arsenic 10/31/22 11/14/22 14 180 OK MW-35 Benzene 10/31/22 11/4/22 4 14 OK MW-35 Beryllium 10/31/22 11/14/22 14 180 OK MW-35 Bicarbonate as CaCO3 10/31/22 11/3/22 3 14 OK MW-35 Cadmium 10/31/22 11/14/22 14 180 OK MW-35 Calcium 10/31/22 11/8/22 8 180 OK MW-35 Carbon Tetrachloride 10/31/22 11/4/22 4 14 OK MW-35 Carbonate as CO3 10/31/22 11/3/22 3 14 OK MW-35 Chloride 10/31/22 11/14/22 14 28 OK MW-35 Chloroform 10/31/22 11/4/22 4 14 OK MW-35 Chloromethane 10/31/22 11/4/22 4 14 OK MW-35 Chromium 10/31/22 11/14/22 14 180 OK MW-35 Cobalt 10/31/22 11/14/22 14 180 OK MW-35 Conner 10/31/22 11/14/22 14 180 OK MW-35 Fluoride 10/31/22 11/14/22 14 28 OK MW-35 Gross Radium Alpha 10/31/22 11/20/22 20 180 OK MW-35 Iron 10/31/22 11/8/22 8 180 OK MW-35 Lead 10/31/22 11/14/22 14 180 OK MW-35 Magnesium 10/31/22 11/8/22 8 180 OK MW-35 Manganese 10/31/22 11/14/22 14 180 OK MW-35 Mercury 10/31/22 11/10/22 10 180 OK MW-35 Methyl Ethyl Ketone 10/31/22 11/4/22 4 14 OK MW-35 Methylene Chloride 10/31/22 11/4/22 4 14 OK MW-35 Molybdenum 10/31/22 11/14/22 14 180 OK MW-35 Naphthalene 10/31/22 11/4/22 4 14 OK MW-35 Nickel 10/31/22 11/14/22 14 180 OK MW-35 Nitrate + Nitrite as N 10/31/22 11/8/22 8 28 OK MW-35 Nitrogen, Ammonia as N 10/31/22 11/14/22 14 28 OK MW-35 Potassium 10/31/22 11/8/22 8 180 OK MW-35 Selenium 10/31/22 11/14/22 14 180 OK MW-35 Silver 10/31/22 11/14/22 14 180 OK MW-35 Sodium 10/31/22 11/8/22 8 180 OK MW-35 Sulfate 10/31/22 11/14/22 14 28 OK MW-35 Tetrahydrofuran 10/31/22 11/4/22 4 14 OK MW-35 Thallium 10/31/22 11/14/22 14 180 OK MW-35 Tin 10/31/22 11/8/22 8 180 OK MW-35 Toluene 10/31/22 11/4/22 4 14 OK MW-35 Total Dissolved Solids 10/31/22 11/4/22 4 7 OK MW-35 Uranium 10/31/22 11/14/22 14 180 OK MW-35 Vanadium 10/31/22 11/14/22 14 180 OK MW-35 Xylenes, total 10/31/22 11/4/22 4 14 OK MW-35 Zinc 10/31/22 11/14/22 14 180 OK MW-36 Acetone 10/11/22 10/19/22 8 14 OK MW-36 Arsenic 10/11/22 10/21/22 10 180 OK MW-36 Benzene 10/11/22 10/19/22 8 14 OK MW-36 Beryllium 10/11/22 10/21/22 10 180 OK MW-36 Bicarbonate as CaCO3 10/11/22 10/19/22 8 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-36 Cadmium 10/11/22 10/21/22 10 180 OK MW-36 Calcium 10/11/22 10/24/22 13 180 OK MW-36 Carbon Tetrachloride 10/11/22 10/19/22 8 14 OK MW-36 Carbonate as CO3 10/11/22 10/19/22 8 14 OK MW-36 Chloride 10/11/22 10/17/22 6 28 OK MW-36 Chloroform 10/11/22 10/19/22 8 14 OK MW-36 Chloromethane 10/11/22 10/19/22 8 14 OK MW-36 Chromium 10/11/22 10/21/22 IO 180 OK MW-36 Cobalt 10/11/22 10/21/22 IO 180 OK MW-36 Coooer 10/11/22 10/21/22 10 180 OK MW-36 Fluoride 10/11/22 10/17/22 6 28 OK MW-36 Gross Radium Alpha 10/11/22 11/14/22 34 180 OK MW-36 Iron 10/11/22 10/24/22 13 180 OK MW-36 Lead 10/11/22 10/21/22 10 180 OK MW-36 Magnesium 10/11/22 10/24/22 13 180 OK MW-36 Manganese 10/11/22 10/21/22 10 180 OK MW-36 Mercury 10/11/22 10/18/22 7 180 OK MW-36 Methyl Ethyl Ketone 10/11/22 10/19/22 8 14 OK MW-36 Methylene Chloride 10/11/22 10/19/22 8 14 OK MW-36 Molybdenum 10/11/22 10/21/22 10 180 OK MW-36 Naphthalene 10/11/22 10/19/22 8 14 OK MW-36 Nickel 10/11/22 10/21/22 10 180 OK MW-36 Nitrate + Nitrite as N 10/11/22 10/18/22 7 28 OK MW-36 Nitrogen, Ammonia as N 10/11/22 10/27/22 16 28 OK MW-36 Potassium 10/11/22 10/24/22 13 180 OK MW-36 Selenium 10/11/22 10/21/22 10 180 OK MW-36 Silver 10/11/22 10/21/22 10 180 OK MW-36 Sodium 10/11/22 10/24/22 13 180 OK MW-36 Sulfate 10/11/22 10/20/22 9 28 OK MW-36 Tetrahydrofuran 10/11/22 10/19/22 8 14 OK MW-36 Thallium 10/11/22 10/21/22 10 180 OK MW-36 Tin 10/11/22 10/24/22 13 180 OK MW-36 Toluene 10/11/22 10/19/22 8 14 OK MW-36 Total Dissolved Solids 10/11/22 10/17/22 6 7 OK MW-36 Uranium 10/11/22 10/21/22 IO 180 OK MW-36 Vanadium 10/11/22 10/21/22 10 180 OK MW-36 Xylenes, total 10/11/22 10/19/22 8 14 OK MW-36 Zinc 10/11/22 10/21/22 10 180 OK MW-37 Acetone 11/1/22 11/4/22 3 14 OK MW-37 Arsenic 11/1/22 11/14/22 13 180 OK MW-37 Benzene 11/1/22 11/4/22 3 14 OK MW-37 Beryllium 11/1/22 11/14/22 13 180 OK MW-37 Bicarbonate as CaCO3 11/1/22 11/3/22 2 14 OK MW-37 Cadmium 11/1/22 11/14/22 13 180 OK MW-37 Calcium 11/1/22 11/8/22 7 180 OK MW-37 Carbon Tetrachloride 11/1/22 11/4/22 3 14 OK MW-37 Carbonate as CO3 11/1/22 11/3/22 2 14 OK MW-37 Chloride 11/1/22 11/14/22 13 28 OK MW-37 Chloroform 11/1/22 11/4/22 3 14 OK MW-37 Chloromethane 11/1/22 11/4/22 3 14 OK MW-37 Chromium 11/1/22 11/14/22 13 180 OK MW-37 Cobalt 11/1/22 11/14/22 13 180 OK MW-37 Copper 11/1/22 11/14/22 13 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-37 Fluoride 11/1/22 11/14/22 13 28 OK MW-37 Gross Radium Alpha 11/1/22 11/20/22 19 180 OK MW-37 Iron 11/1/22 11/8/22 7 180 OK MW-37 Lead 11/1/22 11/14/22 13 180 OK MW-37 Magnesium 11/1/22 11/8/22 7 180 OK MW-37 Manganese 11/1/22 11/14/22 13 180 OK MW-37 Mercury 11/1/22 11/10/22 9 180 OK MW-37 Methyl Ethyl Ketone 11/1/22 11/4/22 3 14 OK MW-37 Methylene Chloride 11/1/22 11/4/22 3 14 OK MW-37 Molybdenum 11/1/22 11/14/22 13 180 OK MW-37 Naphthalene 11/1/22 11/4/22 3 14 OK MW-37 Nickel 11/1/22 11/14/22 13 180 OK MW-37 Nitrate + Nitrite as N 11/1/22 11/8/22 7 28 OK MW-37 Nitrogen, Ammonia as N 11/1/22 11/14/22 13 28 OK MW-37 Potassium 11/1/22 11/8/22 7 180 OK MW-37 Selenium 11/1/22 11/14/22 13 180 OK MW-37 Silver 11/1/22 11/14/22 13 180 OK MW-37 Sodium 11/1/22 11/8/22 7 180 OK MW-37 Sulfate 11/1/22 11/14/22 13 28 OK MW-37 Tetrahydrofuran 11/1/22 11/4/22 3 14 OK MW-37 Thallium 11/1/22 11/14/22 13 180 OK MW-37 Tin 11/1/22 11/8/22 7 180 OK MW-37 Toluene 11/1/22 11/4/22 3 14 OK MW-37 Total Dissolved Solids 11/1/22 11/4/22 3 7 OK MW-37 Uranium 11/1/22 11/14/22 13 180 OK MW-37 Vanadium 11/1/22 11/14/22 13 180 OK MW-37 Xvlenes, total 11/1/22 11/4/22 3 14 OK MW-37 Zinc 11/1/22 11/14/22 13 180 OK MW-38 Acetone 11/1/22 11/4/22 3 14 OK MW-38 Arsenic 11/1/22 11/14/22 13 180 OK MW-38 Benzene 11/1/22 11/4/22 3 14 OK MW-38 Beryllium 11/1/22 11/14/22 13 180 OK MW-38 Bicarbonate as CaCO3 11/1/22 11/3/22 2 14 OK MW-38 Cadmium 11/1/22 11/14/22 13 180 OK MW-38 Calcium 11/1/22 11/8/22 7 180 OK MW-38 Carbon Tetrachloride 11/1/22 11/4/22 3 14 OK MW-38 Carbonate as CO3 11/1/22 11/3/22 2 14 OK MW-38 Chloride 11/1/22 11/14/22 13 28 OK MW-38 Chloroform 11/1/22 11/4/22 3 14 OK MW-38 Chloromethane 11/1/22 11/4/22 3 14 OK MW-38 Chromium 11/1/22 11/14/22 13 180 OK MW-38 Cobalt 11/1/22 11/14/22 13 180 OK MW-38 Cooner 11/1/22 11/14/22 13 180 OK MW-38 Fluoride 11/1/22 11/14/22 13 28 OK MW-38 Gross Radium Alpha 11/1/22 11/20/22 19 180 OK MW-38 Iron 11/1/22 11/8/22 7 180 OK MW-38 Lead 11/1/22 11/14/22 13 180 OK MW-38 Magnesium 11/1/22 11/8/22 7 180 OK MW-38 Manganese 11/1/22 11/14/22 13 180 OK MW-38 Mercury 11/1/22 11/10/22 9 180 OK MW-38 Methyl Ethyl Ketone 11/1/22 11/4/22 3 14 OK MW-38 Methylene Chloride 11/1/22 11/4/22 3 14 OK MW-38 Molybdenum 11/1/22 11/14/22 13 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-38 Naphthalene 11/1/22 11/4/22 3 14 OK MW-38 Nickel 11/1/22 11/14/22 13 180 OK MW-38 Nitrate + Nitrite as N 11/1/22 11/8/22 7 28 OK MW-38 Nitro_gen, Ammonia as N 11/1/22 11/14/22 13 28 OK MW-38 Potassium 11/1/22 11/8/22 7 180 OK MW-38 Selenium 11/1/22 11/14/22 13 180 OK MW-38 Silver 11/1/22 11/14/22 13 180 OK MW-38 Sodium 11/1/22 11/8/22 7 180 OK MW-38 Sulfate 11/1/22 11/14/22 13 28 OK MW-38 Tetrahydrofuran 11/1/22 11/4/22 3 14 OK MW-38 Thallium 11/1/22 11/14/22 13 180 OK MW-38 Tin 11/1/22 11/8/22 7 180 OK MW-38 Toluene 11/1/22 11/4/22 3 14 OK MW-38 Total Dissolved Solids 11/1/22 11/4/22 3 7 OK MW-38 Uranium 11/1/22 11/14/22 13 180 OK MW-38 Vanadium 11/1/22 11/14/22 13 180 OK MW-38 Xylenes, total 11/1/22 11/4/22 3 14 OK MW-38 Zinc 11/1/22 11/14/22 13 180 OK MW-39 Acetone 10/20/22 10/26/22 6 14 OK MW-39 Arsenic 10/20/22 10/26/22 6 180 OK MW-39 Benzene 10/20/22 10/26/22 6 14 OK MW-39 Beryllium 10/20/22 10/26/22 6 180 OK MW-39 Bicarbonate as CaCO3 10/20/22 10/22/22 2 14 OK MW-39 Cadmium 10/20/22 10/26/22 6 180 OK MW-39 Calcium 10/20/22 10/24/22 4 180 OK MW-39 Carbon Tetrachloride 10/20/22 10/26/22 6 14 OK MW-39 Carbonate as CO3 10/20/22 10/22/22 2 14 OK MW-39 Chloride 10/20/22 10/25/22 5 28 OK MW-39 Chloroform 10/20/22 10/26/22 6 14 OK MW-39 Chloromethane 10/20/22 10/26/22 6 14 OK MW-39 Chromium 10/20/22 10/26/22 6 180 OK MW-39 Cobalt 10/20/22 10/26/22 6 180 OK MW-39 Copper 10/20/22 10/26/22 6 180 OK MW-39 Fluoride 10/20/22 11/2/22 13 28 OK MW-39 Iron 10/20/22 10/24/22 4 180 OK MW-39 Lead 10/20/22 10/26/22 6 180 OK MW-39 Ma_gnesium 10/20/22 10/24/22 4 180 OK MW-39 Man_ganese 10/20/22 10/26/22 6 180 OK MW-39 Mercury 10/20/22 10/26/22 6 180 OK MW-39 Methyl Ethyl Ketone 10/20/22 10/26/22 6 14 OK MW-39 Methylene Chloride 10/20/22 10/26/22 6 14 OK MW-39 Molybdenum 10/20/22 10/26/22 6 180 OK MW-39 Naphthalene 10/20/22 10/26/22 6 14 OK MW-39 Nickel 10/20/22 10/26/22 6 180 OK MW-39 Nitrate + Nitrite as N 10/20/22 10/25/22 5 28 OK MW-39 Nitrogen, Ammonia as N 10/20/22 11/2/22 13 28 OK MW-39 Potassium 10/20/22 10/24/22 4 180 OK MW-39 Selenium 10/20/22 10/26/22 6 180 OK MW-39 Silver 10/20/22 10/26/22 6 180 OK MW-39 Sodium 10/20/22 10/24/22 4 180 OK MW-39 Sulfate 10/20/22 11/8/22 19 28 OK MW-39 Tetrahydrofuran 10/20/22 10/26/22 6 14 OK MW-39 Thallium 10/20/22 10/26/22 6 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-39 Tin 10/20/22 10/24/22 4 180 OK MW-39 Toluene 10/20/22 10/26/22 6 14 OK MW-39 Total Dissolved Solids 10/20/22 10/24/22 4 7 OK MW-39 Uranium 10/20/22 10/26/22 6 180 OK MW-39 Vanadium 10/20/22 10/26/22 6 180 OK MW-39 Xylenes, total 10/20/22 10/26/22 6 14 OK MW-39 Zinc 10/20/22 10/26/22 6 180 OK MW-39 Gross Radium Alpha 11/1/22 11/20/22 19 180 OK MW-40 Acetone 10/18/22 10/26/22 8 14 OK MW-40 Arsenic 10/18/22 10/26/22 8 180 OK MW-40 Benzene 10/18/22 10/26/22 8 14 OK MW-40 Beryllium 10/18/22 10/26/22 8 180 OK MW-40 Bicarbonate as CaCO3 10/18/22 10/25/22 7 14 OK MW-40 Cadmium 10/18/22 10/26/22 8 180 OK MW-40 Calcium 10/18/22 10/24/22 6 180 OK MW-40 Carbon Tetrachloride 10/18/22 10/26/22 8 14 OK MW-40 Carbonate as CO3 10/18/22 10/25/22 7 14 OK MW-40 Chloride 10/18/22 10/25/22 7 28 OK MW-40 Chloroform 10/18/22 10/26/22 8 14 OK MW-40 Chloromethane 10/18/22 10/26/22 8 14 OK MW-40 Chromium 10/18/22 10/26/22 8 180 OK MW-40 Cobalt 10/18/22 10/26/22 8 180 OK MW-40 Copper 10/18/22 10/26/22 8 180 OK MW-40 Fluoride 10/18/22 11/2/22 15 28 OK MW-40 Gross Radium Alpha 10/18/22 11/20/22 33 180 OK MW-40 Iron 10/18/22 10/24/22 6 180 OK MW-40 Lead 10/18/22 10/26/22 8 180 OK MW-40 Magnesium 10/18/22 10/24/22 6 180 OK MW-40 Manganese 10/18/22 10/26/22 8 180 OK MW-40 Mercury 10/18/22 10/26/22 8 180 OK MW-40 Methyl Ethyl Ketone 10/18/22 10/26/22 8 14 OK MW-40 Methylene Chloride 10/18/22 10/26/22 8 14 OK MW-40 Molybdenum 10/18/22 10/26/22 8 180 OK MW-40 Naphthalene 10/18/22 10/26/22 8 14 OK MW-40 Nickel 10/18/22 10/26/22 8 180 OK MW-40 Nitrate + Nitrite as N 10/18/22 10/24/22 6 28 OK MW-40 Nitrogen, Ammonia as N 10/18/22 11/2/22 15 28 OK MW-40 Potassium 10/18/22 10/24/22 6 180 OK MW-40 Selenium 10/18/22 10/26/22 8 180 OK MW-40 Silver 10/18/22 10/26/22 8 180 OK MW-40 Sodium 10/18/22 10/24/22 6 180 OK MW-40 Sulfate 10/18/22 10/25/22 7 28 OK MW-40 Tetrahydrofuran 10/18/22 10/26/22 8 14 OK MW-40 Thallium 10/18/22 10/26/22 8 180 OK MW-40 Tin 10/18/22 10/24/22 6 180 OK MW-40 Toluene 10/18/22 10/26/22 8 14 OK MW-40 Total Dissolved Solids 10/18/22 10/24/22 6 7 OK MW-40 Uranium 10/18/22 10/26/22 8 180 OK MW-40 Vanadium 10/18/22 10/26/22 8 180 OK MW-40 Xylenes, total 10/18/22 10/26/22 8 14 OK MW-40 Zinc 10/18/22 10/26/22 8 180 OK MW-65 Acetone 10/13/22 10/19/22 6 14 OK MW-65 Arsenic 10/13/22 10/21/22 8 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-65 Benzene 10/13/22 10/19/22 6 14 OK MW-65 Beryllium 10/13/22 10/21/22 8 180 OK MW-65 Bicarbonate as CaCO3 10/13/22 10/19/22 6 14 OK MW-65 Cadmium 10/13/22 10/21/22 8 180 OK MW-65 Calcium 10/13/22 10/24/22 11 180 OK MW-65 Carbon Tetrachloride 10/13/22 10/19/22 6 14 OK MW-65 Carbonate as CO3 10/13/22 10/19/22 6 14 OK MW-65 Chloride 10/13/22 10/18/22 5 28 OK MW-65 Chloroform 10/13/22 10/19/22 6 14 OK MW-65 Chloromethane 10/13/22 10/19/22 6 14 OK MW-65 Chromium 10/13/22 10/21/22 8 180 OK MW-65 Cobalt 10/13/22 10/21/22 8 180 OK MW-65 Copper 10/13/22 10/21/22 8 180 OK MW-65 Fluoride 10/13/22 10/18/22 5 28 OK MW-65 Gross Radium Alpha 10/13/22 11/14/22 32 180 OK MW-65 Iron 10/13/22 10/24/22 11 180 OK MW-65 Lead 10/13/22 10/21/22 8 180 OK MW-65 Magnesium 10/13/22 10/24/22 11 180 OK MW-65 Manganese 10/13/22 10/21/22 8 180 OK MW-65 Mercury 10/13/22 10/18/22 5 180 OK MW-65 Methyl Ethyl Ketone 10/13/22 10/19/22 6 14 OK MW-65 Methylene Chloride 10/13/22 10/19/22 6 14 OK MW-65 Molybdenum 10/13/22 10/21/22 8 180 OK MW-65 Naphthalene 10/13/22 10/19/22 6 14 OK MW-65 Nickel 10/13/22 10/21/22 8 180 OK MW-65 Nitrate+ Nitrite as N 10/13/22 10/18/22 5 28 OK MW-65 Nitrogen, Ammonia as N 10/13/22 10/27/22 14 28 OK MW-65 Potassium 10/13/22 10/24/22 11 180 OK MW-65 Selenium 10/13/22 10/21/22 8 180 OK MW-65 Silver 10/13/22 10/21/22 8 180 OK MW-65 Sodium 10/13/22 10/24/22 11 180 OK MW-65 Sulfate 10/13/22 10/20/22 7 28 OK MW-65 Tetrahydrofuran 10/13/22 10/19/22 6 14 OK MW-65 Thallium 10/13/22 10/21/22 8 180 OK MW-65 Tin 10/13/22 10/24/22 11 180 OK MW-65 Toluene 10/13/22 10/19/22 6 14 OK MW-65 Total Dissolved Solids 10/13/22 10/17/22 4 7 OK MW-65 Uranium 10/13/22 10/21/22 8 180 OK MW-65 Vanadium 10/13/22 10/21/22 8 180 OK MW-65 Xylenes, total 10/13/22 10/19/22 6 14 OK MW-65 Zinc 10/13/22 10/21/22 8 180 OK MW-70 Acetone 10/31/22 11/4/22 4 14 OK MW-70 Arsenic 10/31/22 11/14/22 14 180 OK MW-70 Benzene 10/31/22 11/4/22 4 14 OK MW-70 Beryllium 10/31/22 11/14/22 14 180 OK MW-70 Bicarbonate as CaCO3 10/31/22 11/3/22 3 14 OK MW-70 Cadmium 10/31/22 11/14/22 14 180 OK MW-70 Calcium 10/31/22 11/8/22 8 180 OK MW-70 Carbon Tetrachloride 10/31/22 11/4/22 4 14 OK MW-70 Carbonate as CO3 10/31/22 11/3/22 3 14 OK MW-70 Chloride 10/31/22 11/14/22 14 28 OK MW-70 Chloroform 10/31/22 11/4/22 4 14 OK MW-70 Chloromethane 10/31/22 11/4/22 4 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-70 Chromium 10/31/22 11/14/22 14 180 OK MW-70 Cobalt 10/31/22 11/14/22 14 180 OK MW-70 Copper 10/31/22 11/14/22 14 180 OK MW-70 Fluoride 10/31/22 11/14/22 14 28 OK MW-70 Gross Radium Alpha 10/31/22 11/20/22 20 180 OK MW-70 Iron 10/31/22 11/8/22 8 180 OK MW-70 Lead 10/31/22 11/14/22 14 180 OK MW-70 Magnesium 10/31/22 11/8/22 8 180 OK MW-70 Manganese 10/31/22 11/14/22 14 180 OK MW-70 Mercury 10/31/22 11/10/22 10 180 OK MW-70 Methyl Ethyl Ketone 10/31/22 11/4/22 4 14 OK MW-70 Methylene Chloride 10/31/22 11/4/22 4 14 OK MW-70 Molybdenum 10/31/22 11/14/22 14 180 OK MW-70 Naphthalene 10/31/22 11/4/22 4 14 OK MW-70 Nickel 10/31/22 11/14/22 14 180 OK MW-70 Nitrate + Nitrite as N 10/31/22 11/8/22 8 28 OK MW-70 Nitrogen, Ammonia as N 10/31/22 11/14/22 14 28 OK MW-70 Potassium 10/31/22 11/8/22 8 180 OK MW-70 Selenium 10/31/22 11/14/22 14 180 OK MW-70 Silver 10/31/22 11/14/22 14 180 OK MW-70 Sodium 10/31/22 11/8/22 8 180 OK MW-70 Sulfate 10/31/22 11/14/22 14 28 OK MW-70 Tetrahydrofuran 10/31/22 11/4/22 4 14 OK MW-70 Thallium 10/31/22 11/14/22 14 180 OK MW-70 Tin 10/31/22 11/8/22 8 180 OK MW-70 Toluene 10/31/22 11/4/22 4 14 OK MW-70 Total Dissolved Solids 10/31/22 11/4/22 4 7 OK MW-70 Uranium 10/31/22 11/14/22 14 180 OK MW-70 Vanadium 10/31/22 11/14/22 14 180 OK MW-70 Xylenes, total 10/31/22 11/4/22 4 14 OK MW-70 Zinc 10/31/22 11/14/22 14 180 OK TW4-24 Acetone 11/1/22 11/4/22 3 14 OK TW4-24 Arsenic 11/1/22 11/14/22 13 180 OK TW4-24 Benzene 11/1/22 11/4/22 3 14 OK TW4-24 Beryllium 11/1/22 11/14/22 13 180 OK TW4-24 Bicarbonate as CaCO3 11/1/22 11/3/22 2 14 OK TW4-24 Cadmium 11/1/22 11/14/22 13 180 OK TW4-24 Calcium 11/1/22 11/8/22 7 180 OK TW4-24 Carbon Tetrachloride 11/1/22 11/4/22 3 14 OK TW4-24 Carbonate as CO3 11/1/22 11/3/22 2 14 OK TW4-24 Chloride 11/1/22 11/14/22 13 28 OK TW4-24 Chloroform 11/1/22 11/4/22 3 14 OK TW4-24 Chloromethane 11/1/22 11/4/22 3 14 OK TW4-24 Chromium 11/1/22 11/14/22 13 180 OK TW4-24 Cobalt 11/1/22 11/14/22 13 180 OK TW4-24 Coooer 11/1/22 11/14/22 13 180 OK TW4-24 Fluoride 11/1/22 11/14/22 13 28 OK TW4-24 Gross Radium Alpha 11/1/22 11/20/22 19 180 OK TW4-24 Iron 11/1/22 11/8/22 7 180 OK TW4-24 Lead 11/1/22 11/14/22 13 180 OK TW4-24· Magnesium 11/1/22 11/8/22 7 180 OK TW4-24 Manganese 11/1/22 11/14/22 13 180 OK TW4-24 Mercury 11/1/22 11/10/22 9 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check TW4-24 Methyl Ethyl Ketone 11/1/22 11/4/22 3 14 OK TW4-24 Methylene Chloride 11/1/22 11/4/22 3 14 OK TW4-24 Molybdenum 11/1/22 11/14/22 13 180 OK TW4-24 Naphthalene 11/1/22 11/4/22 3 14 OK TW4-24 Nickel 11/1/22 11/14/22 13 180 OK TW4-24 Nitrate + Nitrite as N 11/1/22 11/8/22 7 28 OK TW4-24 Nitrogen, Ammonia as N 11/1/22 11/14/22 13 28 OK TW4-24 Potassium 11/1/22 11/8/22 7 180 OK TW4-24 Selenium 11/1/22 11/14/22 13 180 OK TW4-24 Silver 11/1/22 11/14/22 13 180 OK TW4-24 Sodium 11/1/22 11/8/22 7 180 OK TW4-24 Sulfate 11/1/22 11/14/22 13 28 OK TW4-24 Tetrahydrofuran 11/1/22 11/4/22 3 14 OK TW4-24 Thallium I 1/1/22 11/14/22 13 180 OK TW4-24 Tin I 1/1/22 11/8/22 7 180 OK TW4-24 Toluene 11/1/22 11/4/22 3 14 OK TW4-24 Total Dissolved Solids 11/1/22 11/4/22 3 7 OK TW4-24 Uranium 11/1/22 I 1/14/22 13 180 OK TW4-24 Vanadium 11/1/22 11/14/22 13 180 OK TW4-24 Xylenes, total 11/1/22 11/4/22 3 14 OK TW4-24 Zinc 11/1/22 I 1/14/22 13 180 OK G-2B: Accelerated Holding Time Evaluation Allowed Hold Time Hold Time Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) (Days) Check Trip Blank Chloroform 11/10/2022 11/16/2022 6 14 OK Trip Blank Chloroform 12/15/2022 12/19/2022 4 14 OK MW-11 Sulfate 11/8/2022 11/14/2022 6 28 OK MW-11 Chloride 11/8/2022 11/16/2022 8 28 OK MW-11 Manganese 11/8/2022 11/21/2022 13 180 OK MW-11 Nitrate + Nitrite as N 11/8/2022 11/21/2022 13 28 OK MW-11 Total Dissolved Solids 11/8/2022 11/11/2022 3 7 OK MW-11 Sulfate 12/14/2022 12/19/2022 5 28 OK MW-11 Chloride 12/14/2022 12/29/2022 15 28 OK MW-11 Manganese 12/14/2022 12/20/2022 6 180 OK MW-11 Nitrate + Nitrite as N 12/14/2022 12/16/2022 2 28 OK MW-11 Total Dissolved Solids 12/14/2022 12/16/2022 2 7 OK MW-25 Total Dissolved Solids 11/9/2022 11/14/2022 5 7 OK MW-25 Total Dissolved Solids 12/14/2022 12/16/2022 2 7 OK MW-26 Chloride 11/10/2022 11/16/2022 6 28 OK MW-26 Chloroform 11/10/2022 11/16/2022 6 14 OK MW-26 Nitrate + Nitrite as N 11/10/2022 11/21/2022 11 28 OK MW-26 Chloride 12/15/2022 12/29/2022 14 28 OK MW-26 Chloroform 12/15/2022 12/19/2022 4 14 OK MW-26 Nitrate + Nitrite as N 12/15/2022 12/16/2022 1 28 OK MW-30 Chloride 11/9/2022 11/17/2022 8 28 OK MW-30 Uranium 11/9/2022 11/21/2022 12 180 OK MW-30 Selenium 11/9/2022 11/21/2022 12 180 OK MW-30 Nitrate + Nitrite as N 11/9/2022 11/21/2022 12 28 OK MW-30 Chloride 12/13/2022 12/29/2022 16 28 OK MW-30 Uranium 12/13/2022 12/20/2022 7 180 OK MW-30 Selenium 12/13/2022 12/20/2022 7 180 OK MW-30 Nitrate + Nitrite as N 12/13/2022 12/29/2022 16 28 OK MW-31 Sulfate 11/8/2022 11/29/2022 21 28 OK MW-31 Chloride 11/8/2022 11/16/2022 8 28 OK MW-31 Uranium 11/8/2022 11/21/2022 13 180 OK MW-31 Nitrate+ Nitrite as N 11/8/2022 11/21/2022 13 28 OK MW-31 Total Dissolved Solids 11/8/2022 11/11/2022 3 7 OK MW-31 Sulfate 12/13/2022 12/19/2022 6 28 OK MW-31 Chloride 12/13/2022 12/29/2022 16 28 OK MW-31 Uranium 12/13/2022 12/20/2022 7 180 OK MW-31 Nitrate + Nitrite as N 12/13/2022 12/16/2022 3 28 OK MW-31 Total Dissolved Solids 12/13/2022 12/16/2022 3 7 OK MW-65 Chloride 11/9/2022 11/16/2022 7 28 OK MW-65 Uranium 11/9/2022 11/21/2022 12 180 OK MW-65 Selenium 11/9/2022 11/21/2022 12 180 OK MW-65 Nitrate + Nitrite as N 11/9/2022 11/21/2022 12 28 OK MW-65 Chloride 12/13/2022 12/29/2022 16 28 OK MW-65 Uranium 12/13/2022 12/20/2022 7 180 OK MW-65 Selenium 12/13/2022 12/20/2022 7 180 OK MW-65 Nitrate + Nitrite as N 12/13/2022 12/16/2022 3 28 OK G-3A: Quarterly Sample Laboratory Receipt Temperature Check Sample Batch Wells in Batch Temperature GEL597226 MW-05,MW-11,MW-12,MW-14,MW-15,MW-25,MW-NA 26, MW-28, MW-29, MW-30, MW-31, MW-36, MW-65 GEL 598057 MW-0l,MW-03A,MW-17,MW-18,MW-19,MW-22,MW-NA 27, MW-40 MW-02 Resample, MW-20, MW-23, MW-24, MW-24A, MW GEL 599611 32 Resample, MW-35, MW-37, MW-38, MW-39 Resample, NA MW-70, TW4-24 MW-05,MW-11,MW-12,MW-14,MW-15,MW-25,MW- CTF22J1153 26, MW-28, MW-29, MW-30, MW-31, MW-32, MW-36, 2.1 °C MW-65, Trip Blank CTF22J1703 MW-01, MW-02, MW-03A, MW-17, MW-18, MW-19, MW-0.9 °C 22. MW-27, MW-39, MW-40, Trip Blank CTF22K0334 MW-20, MW-23, MW-24, MW-24A, MW-35, MW-37, MW-3.1 °C 38, MW-70, TW4-24, Trip Blank NIA= These shipments contained samples for the analysis of gross alpha or metals only. Per _Table 1 in the approved QAP, samples submitted for gross alpha or metals analyses do not have a sample temperature requirement. G-3B: Accelerated Sample Laboratory Receipt Temperature Check Sample Batch Wells in Batch Temperature CTF 22K09634 -November MW-11, MW-25, MW-26, MW-30, MW-31, MW-65, Trip 0.3 °C Blank CTF 22L1318 -December MW-11, MW-25, MW-26, MW-30, MW-31, MW-65, Trip 0.1 °C Blank G-4A: Quarterly Sample Analytical Method Check Parameter QAPMethod Method Used by Lab Ammonia (as N) A4500-NH3 G or E350.1 E350.1 Nitrate+ Nitrite (as N) E353. l or E353.2 E353.2 Metals E200.7 or E200.8 E200.7 and E200.8 Gross Alpha E900.0 or E900.1 or E903.0 E903.0 voes SW8260B or SW8260C or SW8260D SW8260D Chloride A4500-Cl B or A4500-Cl E or E300.0 E300.0 Fluoride A4500-F C or E300.0 E300.0 Sulfate A4500-SO4 E or E300.0 E300.0 TDS A2540 C A2540C Carbonate as CO3, Bicarbonate as HCO3 A2320B A2320 B Mercury E245.1 or E200.7 or E200.8 E245.l Calcium, Magnesium, Potassium, Sodium E200.7 E200.7 G-4B: Accelerated Sample Analytical Method Check Parameter QAPMethod Method Used by Lab Nitrate+ Nitrite (as N) E353.1 or E353.2 E353.2 Metals E200.7 or E200.8 E200.7 or E200.8 voes SW8260B or SW8260C or SW8260D SW8260D Chloride A4500-CI B or A4500-Cl E or E300.0 E300.0 Sulfate A4500-SO4 E or E300.0 E300.0 TDS A2540 C A2540 C G-5A Quarterly Sample Reporting Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check Trip Blank Acetone 20 ug/L u I 20 OK Trip Blank Benzene l ug/L u 1 1 OK Trip Blank Carbon Tetrachloride 1 ug/L u 1 1 OK Trip Blank Chloroform 1 ug/L u 1 1 OK Trip Blank Chloromethane 1 ug/L u 1 1 OK Trip Blank Methyl Ethyl Ketone 20 ug/L u 1 20 OK Trip Blank Methylene Chloride 1 ug/L u 1 1 OK Trip Blank Naphthalene 1 ug/L u 1 1 OK Trip Blank Tetrahydrofuran 1 ug/L u I I OK Trip Blank Toluene 1 ug/L u 1 1 OK Trip Blank Xylenes, total I ug/L u 1 1 OK Trip Blank Acetone 20 ug/L u 1 20 OK Trip Blank Benzene 1 ug/L u 1 1 OK Trip Blank Carbon Tetrachloride 1 ug/L u 1 1 OK Trip Blank Chloroform 1 ug/L u 1 1 OK Trip Blank Chloromethane 1 ug/L u 1 1 OK Trip Blank Methyl Ethyl Ketone 20 ug/L u 1 20 OK Trip Blank Methylene Chloride I ug/L u I 1 OK Trip Blank Naphthalene 1 ug/L u 1 1 OK Trip Blank Tetrahydrofuran 1 ug/L u 1 1 OK Trip Blank Toluene I ug/L u 1 1 OK Trip Blank Xylenes, total 1 ug/L u 1 1 OK Trip Blank Acetone 20 ug/L u 1 20 OK Trip Blank Benzene 1 ug/L u I 1 OK Trip Blank Carbon Tetrachloride 1 ug/L u 1 1 OK Trip Blank Chloroform 1 ug/L u 1 1 OK Trip Blank Chloromethane 1 ug/L u 1 1 OK Trip Blank Methyl Ethyl Ketone 20 ug/L u 1 20 OK Trip Blank Methylene Chloride 1 ug/L u 1 1 OK Trip Blank Naphthalene 1 ug/L u 1 1 OK Trip Blank Tetrahydrofuran 1 ug/L u 1 1 OK Trip Blank Toluene 1 ug/L u 1 1 OK Trip Blank Xylenes, total 1 ug/L u 1 1 OK MW-01 Acetone 20 ug/L u 1 20 OK MW-01 Arsenic 5 ug/L u 1 5 OK MW-01 Benzene 1 ug/L u 1 1 OK MW-01 Beryllium 0.5 ug/L u 1 0.5 OK MW-01 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-01 Cadmium 0.5 ug/L u 1 0.5 OK MW-01 Calcium 0.2 mg/L 1 0.5 OK MW-01 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-01 Carbonate as CO3 1 mg/L u 1 1 OK MW-01 Chloride 1 mg/L 1 1 OK MW-01 Chloroform 1 ug/L u 1 1 OK MW-01 Chloromethane 1 ug/L u 1 1 OK MW-01 Chromium 25 ug/L u 1 25 OK MW-01 Cobalt 10 ug/L u 1 10 OK MW-01 Coooer 10 ug/L u 1 10 OK MW-01 Fluoride 0.1 mg/L 1 0.1 OK MW-01 Gross Radium Alpha 0.683 pCi/L u 1 1 OK MW-01 Iron 30 ug/L I 30 OK MW-01 Lead 1 ug/L u 1 1 OK MW-01 Magnesium 0.2 mg/L 1 0.5 OK MW-01 Manganese 10 ug/L I 10 OK G-5A . uanerly Sarnp e Reporting Q urut ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-01 Mercury 0.5 ug/L u 1 0.5 OK MW-01 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-01 Methylene Chloride 1 ug/L u 1 1 OK MW-01 Molybdenum 10 ug/L u 1 10 OK MW-01 Naphthalene 1 ug/L u 1 1 OK MW-01 Nickel 20 ug/L u 1 20 OK MW-01 Nitrate + Nitrite as N 0.1 mg/L u 1 0.1 OK MW-01 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-01 Potassium 0.5 mg/L 1 0.5 OK MW-01 Selenium 5 ug/L u 1 5 OK MW-01 Silver 10 ug/L u 1 10 OK MW-01 Sodium 0.5 mg/L 1 0.5 OK MW-01 Sulfate 20 mg/L 20 1 OK MW-01 Tetrahydrofuran 1 ug/L 1 1 OK MW-01 Thallium 0.5 ug/L u 1 0.5 OK MW-01 Tin 100 ug/L u 1 100 OK MW-01 Toluene 1 ug/L u 1 1 OK MW-01 Total Dissolved Solids 20 MG/L 2 10 OK MW-01 Uranium 0.3 ug/L u 1 0.3 OK MW-01 Vanadium 15 ug/L u 1 15 OK MW-01 Xylenes, total 1 ug/L u 1 1 OK MW-01 Zinc 10 ug/L u 1 10 OK MW-02 Acetone 20 ug/L u 1 20 OK MW-02 Arsenic 5 ug/L u 1 5 OK MW-02 Benzene 1 ug/L u 1 1 OK MW-02 Beryllium 0.5 ug/L u 1 0.5 OK MW-02 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-02 Cadmium 0.5 ug/L u 1 0.5 OK MW-02 Calcium 0.2 mg/L 1 0.5 OK MW-02 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-02 Carbonate as CO3 1 mg/L u 1 1 OK MW-02 Chloride 1 mg/L 1 1 OK MW-02 Chloroform 1 ug/L u 1 1 OK MW-02 Chloromethane 1 ug/L u 1 1 OK MW-02 Chromium 25 ug/L u 1 25 OK MW-02 Cobalt 10 ug/L u 1 10 OK MW-02 Cooner 10 ug/L u 1 10 OK MW-02 Fluoride 0.1 mg/L 1 0.1 OK MW-02 Iron 30 ug/L u 1 30 OK MW-02 Lead 1 ug/L u 1 1 OK MW-02 Magnesium 0.2 mg/L 1 0.5 OK MW-02 Manganese 10 ug/L u 1 10 OK MW-02 Mercury 0.5 ug/L u 1 0.5 OK MW-02 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-02 Methylene Chloride 1 ug/L u 1 1 OK MW-02 Molybdenum 10 ug/L u 1 10 OK MW-02 Naphthalene 1 ug/L u 1 1 OK MW-02 Nickel 20 ug/L u 1 20 OK MW-02 Nitrate + Nitrite as N 0.1 mg/L u 1 0.1 OK MW-02 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-02 Potassium 0.5 mg/L 1 0.5 OK MW-02 Selenium 5 ug/L 1 5 OK MW-02 Silver 10 ug/L u 1 10 OK MW-02 Sodium 5 mg/L 10 0.5 OK G-A 5 Q uarter1y amp e I S JR eporung mut ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analvte Limit Units Qualifier Factor Limit Check MW-02 Sulfate 50 mg/L 50 I OK MW-02 Tetrahydrofuran I ug/L u I 1 OK MW-02 Thallium 0.5 ug/L u I 0.5 OK MW-02 Tin 100 ug/L u I 100 OK MW-02 Toluene I ug/L u I 1 OK MW-02 Total Dissolved Solids 20 MG/L 2 10 OK MW-02 Uranium 0.3 ug/L 1 0.3 OK MW-02 Vanadium 15 ug/L u 1 15 OK MW-02 Xylenes, total 1 ug/L u 1 1 OK MW-02 Zinc 10 ug/L u 1 10 OK MW-02 Gross Radium Alpha 0.645 pCi/L 1 1 OK MW-03a Acetone 20 ug/L u 1 20 OK MW-03a Arsenic 5 ug/L u 1 5 OK MW-03a Benzene 1 ug/L u I 1 OK MW-03a Beryllium 0.5 ug/L u I 0.5 OK MW-03a Bicarbonate as CaCO3 1 mg/L I 1 OK MW-03a Cadmium 0.5 ug/L I 0.5 OK MW-03a Calcium 0.2 mg/L 1 0.5 OK MW-03a Carbon Tetrachloride I ug/L u 1 1 OK MW-03a Carbonate as CO3 I mg/L u 1 1 OK MW-03a Chloride 20 mg/L 20 1 OK MW-03a Chloroform 1 ug/L u 1 1 OK MW-03a Chloromethane 1 ug/L u 1 1 OK MW-03a Chromium 25 ug/L u 1 25 OK MW-03a Cobalt 10 ug/L u I 10 OK MW-03a Copper 10 ug/L u I 10 OK MW-03a Fluoride 0.5 mg/L 5 0.1 OK MW-03a Gross Radium Alpha 0.747 pCi/L u I 1 OK MW-03a Iron 30 ug/L u I 30 OK MW-03a Lead 1 ug/L u I 1 OK MW-03a Magnesium 0.2 mg/L I 0.5 OK MW-03a Manganese 10 ug/L 1 10 OK MW-03a Mercury 0.5 ug/L u I 0.5 OK MW-03a Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-03a Methylene Chloride 1 ug/L u I 1 OK MW-03a Molybdenum 10 ug/L u 1 10 OK MW-03a Naphthalene 1 ug/L u I 1 OK MW-03a Nickel 20 ug/L u 1 20 OK MW-03a Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-03a Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-03a Potassium 0.5 mg/L 1 0.5 OK MW-03a Selenium 5 ug/L 1 5 OK MW-03a Silver 10 ug/L u 1 10 OK MW-03a Sodium 5 mg/L 10 0.5 OK MW-03a Sulfate 50 mg/L 50 1 OK MW-03a Tetrahydrofuran I ug/L u I 1 OK MW-03a Thallium 0.5 ug/L u 1 0.5 OK MW-03a Tin 100 ug/L u 1 100 OK MW-03a Toluene 1 ug/L u 1 1 OK MW-03a Total Dissolved Solids 20 MG/L 2 10 OK MW-03a Uranium 0.3 ug/L 1 0.3 OK MW-03a Vanadium 15 ug/L u I 15 OK MW-03a Xylenes, total 1 ug/L u I 1 OK MW-03a Zinc 10 ug/L 1 10 OK G-5A Quarterly Sample Reportmg Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-05 Acetone 20 ug/L u 1 20 OK MW-05 Arsenic 5 ug/L u 1 5 OK MW-05 Benzene 1 ug/L u 1 1 OK MW-05 Beryllium 0.5 ug/L u 1 0.5 OK MW-05 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-05 Cadmium 0.5 ug/L u 1 0.5 OK MW-05 Calcium 0.2 mg/L 1 0.5 OK MW-05 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-05 Carbonate as CO3 1 mg/L u 1 1 OK MW-05 Chloride 1 mg/L 1 1 OK MW-05 Chloroform 1 ug/L u 1 1 OK MW-05 Chloromethane 1 ug/L u 1 1 OK MW-05 Chromium 25 ug/L u 1 25 OK MW-05 Cobalt 10 ug/L u 1 10 OK MW-05 Copper 10 ug/L u 1 10 OK MW-05 Fluoride 0.1 mg/L 1 0.1 OK MW-05 Gross Radium Alpha 0.652 pCi/L u 1 1 OK MW-05 Iron 30 ug/L u 1 30 OK MW-05 Lead 1 ug/L u 1 1 OK MW-05 Magnesium 0.2 mg/L 1 0.5 OK MW-05 Manganese 10 ug/L 1 10 OK MW-05 Mercury 0.5 ug/L u 1 0.5 OK MW-05 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-05 Methylene Chloride 1 ug/L u 1 1 OK MW-05 Molybdenum 10 ug/L u 1 10 OK MW-05 Naphthalene 1 ug/L u 1 1 OK MW-05 Nickel 20 ug/L u 1 20 OK MW-05 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-05 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-05 Potassium 0.5 mg/L 1 0.5 OK MW-05 Selenium 5 ug/L u 1 5 OK MW-05 Silver 10 ug/L u 1 10 OK MW-05 Sodium 0.5 mg/L 1 0.5 OK MW-05 Sulfate 100 mg/L 100 1 OK MW-05 Tetrahydrofuran 1 ug/L 1 1 OK MW-05 Thallium 0.5 ug/L u 1 0.5 OK MW-05 Tin 100 ug/L u 1 100 OK MW-05 Toluene 1 ug/L u 1 1 OK MW-05 Total Dissolved Solids 20 MG/L 2 10 OK MW-05 Uranium 0.3 ug/L 1 0.3 OK MW-05 Vanadium 15 ug/L u 1 15 OK MW-05 Xylenes, total 1 ug/L u 1 1 OK MW-05 Zinc 10 ug/L u 1 10 OK MW-11 Acetone 20 ug/L u 1 20 OK MW-11 Arsenic 5 ug/L u 1 5 OK MW-11 Benzene 1 ug/L u 1 1 OK MW-11 Beryllium 0.5 ug/L u 1 0.5 OK MW-11 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-11 Cadmium 0.5 ug/L u 1 0.5 OK MW-11 Calcium 0.2 mg/L 1 0.5 OK MW-11 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-11 Carbonate as CO3 1 mg/L u 1 1 OK MW-11 Chloride 1 mg/L 1 1 OK MW-11 Chloroform 1 ug/L u 1 1 OK h k G-5A Quarlerly Sample Reporung Limit C ec Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-11 Chloromethane I ug/L u I 1 OK MW-11 Chromium 25 ug/L u 1 25 OK MW-11 Cobalt 10 ug/L u 1 10 OK MW-11 Copper 10 ug/L u 1 10 OK MW-II Fluoride 0.1 mg/L 1 0.1 OK MW-II Gross Radium Alpha 0.599 pCi/L u 1 1 OK MW-11 Iron 30 ug/L u 1 30 OK MW-11 Lead 1 ug/L u 1 1 OK MW-11 Magnesium 0.2 mg/L 1 0.5 OK MW-11 Manganese 10 ug/L 1 10 OK MW-11 Mercury 0.5 ug/L u 1 0.5 OK MW-11 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-11 Methylene Chloride I ug/L u 1 1 OK MW-11 Molybdenum 10 ug/L u I 10 OK MW-11 Naphthalene I ug/L u I 1 OK MW-11 Nickel 20 ug/L u I 20 OK MW-11 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-11 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-11 Potassium 0.5 mg/L 1 0.5 OK MW-11 Selenium 5 ug/L I 5 OK MW-11 Silver 10 ug/L u I 10 OK MW-11 Sodium 5 mg/L 10 0.5 OK MW-11 Sulfate 100 mg/L 100 1 OK MW-11 Tetrahydrofuran 1 ug/L u 1 1 OK MW-11 Thallium 0.5 ug/L u I 0.5 OK MW-11 Tin 100 ug/L u I 100 OK MW-11 Toluene 1 ug/L u 1 I OK MW-11 Total Dissolved Solids 20 MG/L 2 10 OK MW-11 Uranium 0.3 ug/L 1 0.3 OK MW-11 Vanadium 15 ug/L u I 15 OK MW-11 Xylenes, total 1 ug/L u l I OK MW-11 Zinc 10 ug/L u l IO OK MW-12 Acetone 20 ug/L u 1 20 OK MW-12 Arsenic 5 ug/L u 1 5 OK MW-12 Benzene 1 ug/L u 1 1 OK MW-12 Beryllium 0.5 ug/L u I 0.5 OK MW-12 Bicarbonate as CaCO3 1 mg/L I 1 OK MW-12 Cadmium 0.5 ug/L u 1 0.5 OK MW-12 Calcium 0.2 mg/L I 0.5 OK MW-12 Carbon Tetrachloride 1 ug/L u I I OK MW-12 Carbonate as CO3 I mg/L u 1 I OK MW-12 Chloride I mg/L 1 I OK MW-12 Chloroform 1 ug/L u 1 l OK MW-12 Chloromethane 1 ug/L u 1 1 OK MW-12 Chromium 25 ug/L u 1 25 OK MW-12 Cobalt 10 ug/L u 1 IO OK MW-12 Copper IO ug/L u 1 IO OK MW-12 Fluoride 0.1 mg/L 1 0.1 OK MW-12 Gross Radium Alpha 0.631 pCi/L u 1 l OK MW-12 Iron 30 ug/L u 1 30 OK MW-12 Lead 1 ug/L u I 1 OK MW-12 Magnesium 0.2 mg/L 1 0.5 OK MW-12 Manganese 10 ug/L 1 10 OK MW-12 Mercury 0.5 ug/L u 1 0.5 OK G5AQ -I S l R uarteriy amp e eportm.£{ 1m1t ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-12 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-12 Methylene Chloride I ug/L u 1 1 OK MW-12 Molybdenum 10 ug/L u 1 10 OK MW-12 Naphthalene 1 ug/L u 1 1 OK MW-12 Nickel 20 ug/L u 1 20 OK MW-12 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-12 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-12 Potassium 0.5 mg/L 1 0.5 OK MW-12 Selenium 5 ug/L 1 5 OK MW-12 Silver 10 ug/L u 1 10 OK MW-12 Sodium 0.5 mg/L 1 0.5 OK MW-12 Sulfate 100 mg/L 100 1 OK MW-12 Tetrahydrofuran 1 ug/L 1 1 OK MW-12 Thallium 0.5 ug/L u 1 0.5 OK MW-12 Tin 100 ug/L u 1 100 OK MW-12 Toluene 1 ug/L u 1 1 OK MW-12 Total Dissolved Solids 20 MG/L 2 10 OK MW-12 Uranium 0.3 ug/L 1 0.3 OK MW-12 Vanadium 15 ug/L u 1 15 OK MW-12 Xylenes, total 1 ug/L u 1 1 OK MW-12 Zinc 10 ug/L u 1 10 OK MW-14 Acetone 20 ug/L u 1 20 OK MW-14 Arsenic 5 ug/L u 1 5 OK MW-14 Benzene 1 ug/L u 1 1 OK MW-14 Beryllium 0.5 ug/L u 1 0.5 OK MW-14 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-14 Cadmium 0.5 ug/L 1 0.5 OK MW-14 Calcium 0.2 mg/L 1 0.5 OK MW-14 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-14 Carbonate as CO3 1 mg/L u 1 1 OK MW-14 Chloride 1 mg/L 1 1 OK MW-14 Chloroform 1 ug/L u 1 1 OK MW-14 Chloromethane 1 ug/L u 1 1 OK MW-14 Chromium 25 ug/L u 1 25 OK MW-14 Cobalt 10 ug/L u 1 10 OK MW-14 Coooer 10 ug/L u 1 10 OK MW-14 Fluoride 0.1 mg/L u 1 0.1 OK MW-14 Gross Radium Alpha 0.771 pCi/L u 1 1 OK MW-14 Iron 30 ug/L u 1 30 OK MW-14 Lead 1 ug/L u 1 1 OK MW-14 Magnesium 0.2 mg/L 1 0.5 OK MW-14 Manganese 10 ug/L 1 10 OK MW-14 Mercury 0.5 ug/L u 1 0.5 OK MW-14 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-14 Methylene Chloride 1 ug/L u 1 1 OK MW-14 Molybdenum 10 ug/L u 1 10 OK MW-14 Naphthalene 1 ug/L u 1 1 OK MW-14 Nickel 20 ug/L u 1 20 OK MW-14 Nitrate + Nitrite as N 0.1 mg/L u 1 0.1 OK MW-14 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-14 Potassium 0.5 mg/L 1 0.5 OK MW-14 Selenium 5 ug/L u 1 5 OK MW-14 Silver 10 ug/L u 1 10 OK MW-14 Sodium 0.5 mg/L 1 0.5 OK G5AQ -I S I R uarter1y amp. e eporttng mut ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-14 Sulfate 100 mg/L 100 1 OK MW-14 Tetrahydrofuran 1 ug/L u 1 1 OK MW-14 Thallium 0.5 ug/L u 1 0.5 OK MW-14 Tin 100 ug/L u 1 100 OK MW-14 Toluene 1 ug/L u 1 1 OK MW-14 Total Dissolved Solids 20 MG/L 2 10 OK MW-14 Uranium 0.3 ug/L 1 0.3 OK MW-14 Vanadium 15 ug/L u 1 15 OK MW-14 Xylenes, total 1 ug/L u 1 1 OK MW-14 Zinc 10 ug/L 1 10 OK MW-15 Acetone 20 ug/L u 1 20 OK MW-15 Arsenic 5 ug/L u 1 5 OK MW-15 Benzene 1 ug/L u 1 1 OK MW-15 Beryllium 0.5 ug/L u 1 0.5 OK MW-15 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-15 Cadmium 0.5 ug/L u 1 0.5 OK MW-15 Calcium 0.2 mg/L 1 0.5 OK MW-15 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-15 Carbonate as CO3 1 mg/L u 1 1 OK MW-15 Chloride 1 mg/L 1 1 OK MW-15 Chloroform 1 ug/L u 1 1 OK MW-15 Chloromethane 1 ug/L u 1 1 OK MW-15 Chromium 25 ug/L u 1 25 OK MW-15 Cobalt 10 ug/L u 1 10 OK MW-15 Copper 10 ug/L u 1 10 OK MW-15 Fluoride 0.1 mg/L u 1 0.1 OK MW-15 Gross Radium Alpha 0.881 pCi/L u 1 1 OK MW-15 Iron 30 ug/L u 1 30 OK MW-15 Lead 1 ug/L u 1 I OK MW-15 Magnesium 0.2 mg/L 1 0.5 OK MW-15 Manganese 10 ug/L u 1 10 OK MW-15 Mercury 0.5 ug/L u 1 0.5 OK MW-15 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-15 Methylene Chloride 1 ug/L u 1 1 OK MW-15 Molybdenum 10 ug/L u 1 10 OK MW-15 Naphthalene 1 ug/L u 1 1 OK MW-15 Nickel 20 ug/L u 1 20 OK MW-15 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-15 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-15 Potassium 0.5 mg/L 1 0.5 OK MW-15 Selenium 5 ug/L 1 5 OK MW-15 Silver 10 ug/L u 1 10 OK MW-15 Sodium 5 mg/L 10 0.5 OK MW-15 Sulfate 100 mg/L 100 1 OK MW-15 Tetrahydrofuran 1 ug/L u 1 1 OK MW-15 Thallium 0.5 ug/L u 1 0.5 OK MW-15 Tin 100 ug/L u 1 100 OK MW-15 Toluene 1 ug/L u 1 1 OK MW-15 Total Dissolved Solids 20 MG/L 2 10 OK MW-15 Uranium 0.3 ug/L 1 0.3 OK MW-15 Vanadium 15 ug/L u 1 15 OK MW-15 Xylenes, total 1 ug/L u 1 1 OK MW-15 Zinc 10 ug/L u 1 10 OK MW-17 Acetone 20 ug/L u 1 20 OK G5AQ -uarter y amp e l S I R epornng urut ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-17 Arsenic 5 ug/L u I 5 OK MW-17 Benzene I ug/L u 1 1 OK MW-17 Beryllium 0.5 ug/L u I 0.5 OK MW-17 Bicarbonate as CaCO3 I mg/L I I OK MW-17 Cadmium 0.5 ug/L u I 0.5 OK MW-17 Calcium 0.2 mg/L I 0.5 OK MW-17 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-17 Carbonate as CO3 I mg/L u I I OK MW-17 Chloride 20 mg/L 20 I OK MW-17 Chloroform I ug/L u 1 I OK MW-17 Chloromethane 1 ug/L u 1 1 OK MW-17 Chromium 25 ug/L u 1 25 OK MW-17 Cobalt IO ug/L u I IO OK MW-17 Copper 10 ug/L u I 10 OK MW-17 Fluoride 0.1 mg/L 1 0.1 OK MW-17 Gross Radium Alpha 0.909 pCi/L u 1 1 OK MW-17 Iron 30 ug/L u 1 30 OK MW-17 Lead 1 ug/L u 1 1 OK MW-17 Magnesium 0.2 mg/L 1 0.5 OK MW-17 Manganese 10 ug/L 1 IO OK MW-17 Mercury 0.5 ug/L u 1 0.5 OK MW-17 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-17 Methylene Chloride 1 ug/L u 1 1 OK MW-17 Molybdenum IO ug/L u 1 IO OK MW-17 Naphthalene 1 ug/L u 1 1 OK MW-17 Nickel 20 ug/L u 1 20 OK MW-17 Nitrate+ Nitrite as N 0.1 mg/L 1 0.1 OK MW-17 Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-17 Potassium 0.5 mg/L I 0.5 OK MW-17 Selenium 5 ug/L 1 5 OK MW-17 Silver IO ug/L u 1 IO OK MW-17 Sodium 0.5 mg/L 1 0.5 OK MW-17 Sulfate 20 mg/L 20 1 OK MW-17 Tetrahydrofuran 1 ug/L u 1 1 OK MW-17 Thallium 0.5 ug/L u 1 0.5 OK MW-17 Tin 100 ug/L u 1 100 OK MW-17 Toluene 1 ug/L u 1 1 OK MW-17 Total Dissolved Solids 20 MG/L 2 IO OK MW-17 Uranium 0.3 ug/L 1 0.3 OK MW-17 Vanadium 15 ug/L u 1 15 OK MW-17 Xylenes, total 1 ug/L u 1 1 OK MW-17 Zinc IO ug/L u 1 IO OK MW-18 Acetone 20 ug/L u 1 20 OK MW-18 Arsenic 5 ug/L u 1 5 OK MW-18 Benzene 1 ug/L u 1 1 OK MW-18 Beryllium 0.5 ug/L u 1 0.5 OK MW-18 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-18 Cadmium 0.5 ug/L u 1 0.5 OK MW-18 Calcium 0.2 mg/L 1 0.5 OK MW-18 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-18 Carbonate as CO3 1 mg/L u 1 1 OK MW-18 Chloride 20 mg/L 20 1 OK MW-18 Chloroform 1 ug/L u 1 1 OK MW-18 Chloromethane 1 ug/L u 1 1 OK G5AQ -uarter1y ampe I S IR eportm~ nrut ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-18 Chromium 25 u.11;/L u I 25 OK MW-18 Cobalt IO u.!?;IL u 1 IO OK MW-18 Coooer 10 ug/L u I 10 OK MW-18 Fluoride 0.1 mg/L I 0.1 OK MW-18 Gross Radium Alpha 0.628 pCi/L u I I OK MW-18 Iron 30 ug/L I 30 OK MW-18 Lead 1 ug/L u 1 1 OK MW-18 Magnesium 0.2 mg/L 1 0.5 OK MW-18 Manganese 10 ug/L 1 10 OK MW-18 Mercury 0.5 ug/L u 1 0.5 OK MW-18 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-18 Methylene Chloride 1 ug/L u I I OK MW-18 Molybdenum 10 u.!?;IL u I 10 OK MW-18 Naphthalene I ug/L u 1 1 OK MW-18 Nickel 20 ug/L u 1 20 OK MW-18 Nitrate + Nitrite as N 0.1 mg/L u I 0.1 OK MW-18 Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-18 Potassium 0.5 mg/L 1 0.5 OK MW-18 Selenium 5 ug/L u 1 5 OK MW-18 Silver 10 ug/L u 1 10 OK MW-18 Sodium 0.5 mg/L I 0.5 OK MW-18 Sulfate 20 mg/L 20 I OK MW-18 Tetrahydrofuran 1 ug/L u 1 I OK MW-18 Thallium 0.5 u.!?;IL 1 0.5 OK MW-18 Tin 100 ug/L u 1 100 OK MW-18 Toluene 1 ug/L u 1 1 OK MW-18 Total Dissolved Solids 20 MG/L 2 10 OK MW-18 Uranium 0.3 ug/L I 0.3 OK MW-18 Vanadium 15 ug/L u I 15 OK MW-18 Xylenes, total 1 ug/L u 1 1 OK MW-18 Zinc 10 u.!?;IL u 1 10 OK MW-19 Acetone 20 ug/L u 1 20 OK MW-19 Arsenic 5 ug/L u 1 5 OK MW-19 Benzene I ug/L u 1 1 OK MW-19 Beryllium 0.5 ug/L u I 0.5 OK MW-19 Bicarbonate as CaCO3 I mg/L I I OK MW-19 Cadmium 0.5 ug/L u 1 0.5 OK MW-19 Calcium 0.2 mg/L 1 0.5 OK MW-19 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-19 Carbonate as CO3 1 mg/L u 1 1 OK MW-19 Chloride 20 mg/L 20 1 OK MW-19 Chloroform 1 ug/L u I 1 OK MW-19 Chloromethane 1 ug/L u 1 1 OK MW-19 Chromium 25 ug/L u I 25 OK MW-19 Cobalt 10 u.!?;IL u I 10 OK MW-19 Copper 10 ug/L u 1 10 OK MW-19 Fluoride 0.2 mg/L 2 0.1 OK MW-19 Gross Radium Alpha 0.676 pCi/L u 1 1 OK MW-19 Iron 30 ug/L u I 30 OK MW-19 Lead 1 ug/L u 1 1 OK MW-19 Magnesium 0.2 mg/L 1 0.5 OK MW-19 Manganese 10 u.!?;IL u I 10 OK MW-19 Mercury 0.5 ug/L u 1 0.5 OK MW-19 Methyl Ethyl Ketone 20 ug/L u 1 20 OK G5AQ -uarter1y amp e eporttng urut ec I S l R L" . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-19 Methylene Chloride 1 ug/L u 1 1 OK MW-19 Molybdenum 10 ug/L u 1 10 OK MW-19 Naphthalene I ug/L u 1 1 OK MW-19 Nickel 20 ug/L u 1 20 OK MW-19 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-19 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-19 Potassium 0.5 mg/L 1 0.5 OK MW-19 Selenium 5 ug/L 1 5 OK MW-19 Silver 10 ug/L u 1 10 OK MW-19 Sodium 0.5 mg/L 1 0.5 OK MW-19 Sulfate 20 mg/L 20 1 OK MW-19 Tetrahydrofuran 1 ug/L u 1 1 OK MW-19 Thallium 0.5 ug/L u 1 0.5 OK MW-19 Tin 100 ug/L u 1 100 OK MW-19 Toluene 1 ug/L u 1 1 OK MW-19 Total Dissolved Solids 20 MG/L 2 10 OK MW-19 Uranium 0.3 ug/L 1 0.3 OK MW-19 Vanadium 15 ug/L u 1 15 OK MW-19 Xylenes, total 1 ug/L u 1 1 OK MW-19 Zinc 10 ug/L u 1 10 OK MW-20 Acetone 20 ug/L u 1 20 OK MW-20 Arsenic 5 ug/L u 1 5 OK MW-20 Benzene 1 ug/L u 1 1 OK MW-20 Beryllium 0.5 ug/L u 1 0.5 OK MW-20 Bicarbonate as CaCO3 1 mg/L I 1 OK MW-20 Cadmium 0.5 ug/L u 1 0.5 OK MW-20 Calcium 0.2 mg/L 1 0.5 OK MW-20 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-20 Carbonate as CO3 1 mg/L u I 1 OK MW-20 Chloride 1 mg/L 1 1 OK MW-20 Chloroform 1 ug/L u I 1 OK MW-20 Chloromethane I ug/L u I 1 OK MW-20 Chromium 25 ug/L u 1 25 OK MW-20 Cobalt 10 ug/L u I 10 OK MW-20 Copper 10 ug/L u 1 10 OK MW-20 Fluoride 0.1 mg/L 1 0.1 OK MW-20 Gross Radium Alpha 0.585 pCi/L u 1 1 OK MW-20 Iron 30 ug/L u 1 30 OK MW-20 Lead I ug/L u 1 1 OK MW-20 Magnesium 0.2 mg/L 1 0.5 OK MW-20 Manganese 10 ug/L u 1 10 OK MW-20 Mercury 0.5 ug/L u 1 0.5 OK MW-20 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-20 Methylene Chloride 1 ug/L u I 1 OK MW-20 Molybdenum 10 ug/L 1 10 OK MW-20 Naphthalene 1 ug/L u I 1 OK MW-20 Nickel 20 ug/L u I 20 OK MW-20 Nitrate + Nitrite as N 2 mg/L 20 0.1 OK MW-20 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-20 Potassium 0.5 mg/L 1 0.5 OK MW-20 Selenium 5 ug/L 1 5 OK MW-20 Silver 10 ug/L u 1 10 OK MW-20 Sodium 5 mg/L 10 0.5 OK MW-20 Sulfate 50 mg/L 50 1 OK G5AQ -1 S I R uarteriy amp e eporttng lffilt ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-20 Tetrahydrofuran I ug/L u I 1 OK MW-20 Thallium 0.5 ug/L u 1 0.5 OK MW-20 Tin 100 ug/L u 1 100 OK MW-20 Toluene 1 ug/L u 1 1 OK MW-20 Total Dissolved Solids 20 MG/L 2 10 OK MW-20 Uranium 0.3 ug/L 1 0.3 OK MW-20 Vanadium 15 ug/L u I 15 OK MW-20 Xylenes, total I ug/L u 1 1 OK MW-20 Zinc 10 ug/L u I 10 OK MW-22 Acetone 20 ug/L u 1 20 OK MW-22 Arsenic 5 ug/L u I 5 OK MW-22 Benzene 1 ug/L u I 1 OK MW-22 Beryllium 0.5 ug/L 1 0.5 OK MW-22 Bicarbonate as CaCO3 I mg/L u 1 1 OK MW-22 Cadmium 0.5 ug/L 1 0.5 OK MW-22 Calcium 0.2 mg/L 1 0.5 OK MW-22 Carbon Tetrachloride I ug/L u 1 1 OK MW-22 Carbonate as CO3 1 mg/L u I 1 OK MW-22 Chloride 20 mg/L 20 I OK MW-22 Chloroform 1 ug/L u 1 1 OK MW-22 Chloromethane 1 ug/L u 1 1 OK MW-22 Chromium 25 ug/L u 1 25 OK MW-22 Cobalt 10 ug/L I 10 OK MW-22 Cooner 10 ug/L 1 10 OK MW-22 Fluoride 0.5 mg/L 5 0.1 OK MW-22 Gross Radium Alpha 0.756 pCi/L I 1 OK MW-22 Iron 30 ug/L 1 30 OK MW-22 Lead 1 ug/L 1 1 OK MW-22 Magnesium 0.2 mg/L I 0.5 OK MW-22 Manganese 10 ug/L 1 10 OK MW-22 Mercury 0.5 ug/L u 1 0.5 OK MW-22 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-22 Methylene Chloride I ug/L u I 1 OK MW-22 Molybdenum 10 ug/L 1 10 OK MW-22 Naphthalene 1 ug/L u 1 1 OK MW-22 Nickel 20 ug/L 1 20 OK MW-22 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-22 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-22 Potassium 0.5 mg/L I 0.5 OK MW-22 Selenium 5 ug/L I 5 OK MW-22 Silver 10 ug/L u I 10 OK MW-22 Sodium 0.5 mg/L I 0.5 OK MW-22 Sulfate 100 mg/L 100 I OK MW-22 Tetrahydrofuran I ug/L u I I OK MW-22 Thallium 0.5 ug/L I 0.5 OK MW-22 Tin 100 ug/L u I 100 OK MW-22 Toluene 1 ug/L u I 1 OK MW-22 Total Dissolved Solids 50 MG/L 2 10 OK MW-22 Uranium 0.3 ug/L 1 0.3 OK MW-22 Vanadium 15 ug/L u 1 15 OK MW-22 Xylenes, total 1 ug/L u 1 1 OK MW-22 Zinc 10 ug/L 1 10 OK MW-23 Acetone 20 ug/L u 1 20 OK MW-23 Arsenic 5 ug/L u 1 5 OK G5AQ -I S I R uarter1y amp e eoorung mut ec L" . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-23 Benzene 1 ug/L u 1 1 OK MW-23 Beryllium 0.5 ug/L u 1 0.5 OK MW-23 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-23 Cadmium 0.5 ug/L u 1 0.5 OK MW-23 Calcium 0.2 mg/L 1 0.5 OK MW-23 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-23 Carbonate as CO3 1 mg/L u 1 1 OK MW-23 Chloride 1 mg/L 1 1 OK MW-23 Chloroform 1 ug/L u 1 1 OK MW-23 Chloromethane 1 ug/L u 1 1 OK MW-23 Chromium 25 ug/L u 1 25 OK MW-23 Cobalt IO ug/L u l IO OK MW-23 Copper IO ug/L u 1 IO OK MW-23 Fluoride 0.1 mg/L 1 0.1 OK MW-23 Gross Radium Alpha 0.727 pCi/L u 1 1 OK MW-23 Iron 30 ug/L u 1 30 OK MW-23 Lead 1 ug/L u 1 1 OK MW-23 Magnesium 0.2 mg/L 1 0.5 OK MW-23 Manganese IO ug/L u 1 IO OK MW-23 Mercury 0.5 ug/L u 1 0.5 OK MW-23 Methyl Ethyl Ketone 20 ug/L u l 20 OK MW-23 Methylene Chloride 1 ug/L u 1 1 OK MW-23 Molybdenum 10 ug/L u 1 IO OK MW-23 Naphthalene 1 ug/L u 1 1 OK MW-23 Nickel 20 ug/L u 1 20 OK MW-23 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-23 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-23 Potassium 0.5 mg/L l 0.5 OK MW-23 Selenium 5 ug/L u 1 5 OK MW-23 Silver IO ug/L u 1 IO OK MW-23 Sodium 0.5 mg/L 1 0.5 OK MW-23 Sulfate 50 mg/L 50 1 OK MW-23 Tetrahydrofuran 1 ug/L u 1 1 OK MW-23 Thallium 0.5 ug/L u l 0.5 OK MW-23 Tin 100 ug/L u 1 100 OK MW-23 Toluene 1 ug/L u 1 1 OK MW-23 Total Dissolved Solids 20 MG/L 2 IO OK MW-23 Uranium 0.3 ug/L 1 0.3 OK MW-23 Vanadium 15 ug/L u 1 15 OK MW-23 Xylenes, total 1 ug/L u 1 1 OK MW-23 Zinc 10 ug/L u 1 10 OK MW-24 Acetone 20 ug/L u 1 20 OK MW-24 Arsenic 5 ug/L u 1 5 OK MW-24 Benzene 1 ug/L u 1 1 OK MW-24 Beryllium 0.5 ug/L 1 0.5 OK MW-24 Bicarbonate as CaCO3 I mg/L u I 1 OK MW-24 Cadmium 0.5 ug/L 1 0.5 OK MW-24 Calcium 0.2 mg/L I 0.5 OK MW-24 Carbon Tetrachloride I ug/L u I 1 OK MW-24 Carbonate as CO3 1 mg/L u 1 I OK MW-24 Chloride I mg/L 1 I OK MW-24 Chloroform 1 ug/L u 1 1 OK MW-24 Chloromethane 1 ug/L u 1 1 OK MW-24 Chromium 25 ug/L u I 25 OK G5AQ -I S I R uarter1y amp e eportm.2. 1m1t ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-24 Cobalt 10 ug/L 1 10 OK MW-24 Cooner 10 ug/L 1 10 OK MW-24 Fluoride 0.1 mg/L 1 0.1 OK MW-24 Gross Radium Alpha 0.71 pCi/L 1 1 OK MW-24 Iron 30 ug/L u 1 30 OK MW-24 Lead 1 ug/L 1 1 OK MW-24 Magnesium 0.2 mg/L 1 0.5 OK MW-24 Manganese 10 ug/L 10 10 OK MW-24 Mercury 0.5 ug/L u 1 0.5 OK MW-24 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-24 Methylene Chloride 1 ug/L u 1 1 OK MW-24 Molybdenum 10 ug/L u 1 10 OK MW-24 Naphthalene 1 ug/L u 1 1 OK MW-24 Nickel 20 ug/L 1 20 OK MW-24 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-24 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-24 Potassium 0.5 mg/L 1 0.5 OK MW-24 Selenium 5 ug/L 1 5 OK MW-24 Silver 10 ug/L u 1 10 OK MW-24 Sodium 0.5 mg/L 1 0.5 OK MW-24 Sulfate 50 mg/L 50 1 OK MW-24 Tetrahydrofuran 1 ug/L u 1 1 OK MW-24 Thallium 0.5 ug/L 1 0.5 OK MW-24 Tin 100 ug/L u 1 100 OK MW-24 Toluene 1 ug/L u 1 1 OK MW-24 Total Dissolved Solids 20 MG/L 2 10 OK MW-24 Uranium 0.3 ug/L 1 0.3 OK MW-24 Vanadium 15 ug/L u 1 15 OK MW-24 Xylenes, total 1 ug/L u 1 1 OK MW-24 Zinc 10 ug/L 1 10 OK MW-24A Acetone 20 ug/L u 1 20 OK MW-24A Arsenic 5 ug/L u 1 5 OK MW-24A Benzene 1 ug/L u 1 1 OK MW-24A Beryllium 0.5 ug/L 1 0.5 OK MW-24A Bicarbonate as CaCO3 1 mg/L u 1 1 OK MW-24A Cadmium 0.5 ug/L 1 0.5 OK MW-24A Calcium 0.2 mg/L 1 0.5 OK MW-24A Carbon Tetrachloride 1 ug/L u 1 1 OK MW-24A Carbonate as CO3 1 mg/L u 1 1 OK MW-24A Chloride 1 mg/L 1 1 OK MW-24A Chloroform 1 ug/L u 1 1 OK MW-24A Chloromethane 1 ug/L u 1 1 OK MW-24A Chromium 25 ug/L u 1 25 OK MW-24A Cobalt 10 ug/L 1 10 OK MW-24A Copper 10 ug/L 1 10 OK MW-24A Fluoride 0.1 mg/L 1 0.1 OK MW-24A Gross Radium Alpha 0.531 pCi/L 1 1 OK MW-24A Iron 30 ug/L u 1 30 OK MW-24A Lead 1 ug/L u 1 1 OK MW-24A Magnesium 0.2 mg/L 1 0.5 OK MW-24A Manganese 10 ug/L 10 10 OK MW-24A Mercury 0.5 ug/L u 1 0.5 OK MW-24A Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-24A Methylene Chloride 1 ug/L u 1 1 OK G5AQ -I S l R uarter1y amp e L' . h k eporLmg 1m1t C ec Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-24A Molybdenum 10 ug/L u I 10 OK MW-24A Naphthalene I ug/L u I I OK MW-24A Nickel 20 ug/L I 20 OK MW-24A Nitrate + Nitrite as N 0.1 mg/L I 0.1 OK MW-24A Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-24A Potassium 0.5 mg/L I 0.5 OK MW-24A Selenium 5 ug/L I 5 OK MW-24A Silver 10 ug/L u I 10 OK MW-24A Sodium 0.5 mg/L I 0.5 OK MW-24A Sulfate 50 mg/L 50 I OK MW-24A Tetrahvdrofuran I ug/L u I I OK MW-24A Thallium 0.5 ug/L I 0.5 OK MW-24A Tin 100 ug/L u 1 100 OK MW-24A Toluene 1 ug/L u I I OK MW-24A Total Dissolved Solids 20 MG/L 2 10 OK MW-24A Uranium 0.3 ug/L 1 0.3 OK MW-24A Vanadium 15 ug/L u 1 15 OK MW-24A Xylenes, total 1 ug/L u I I OK MW-24A Zinc 10 ug/L 1 10 OK MW-25 Acetone 20 ug/L u I 20 OK MW-25 Arsenic 5 ug/L u I 5 OK MW-25 Benzene 1 ug/L u 1 1 OK MW-25 Beryllium 0.5 ug/L u 1 0.5 OK MW-25 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-25 Cadmium 0.5 ug/L 1 0.5 OK MW-25 Calcium 0.2 mg/L 1 0.5 OK MW-25 Carbon Tetrachloride 1 ug/L u I 1 OK MW-25 Carbonate as CO3 1 mg/L u I I OK MW-25 Chloride 1 mg/L 1 I OK MW-25 Chloroform 1 ug/L u 1 1 OK MW-25 Chloromethane I ug/L u 1 I OK MW-25 Chromium 25 ug/L u I 25 OK MW-25 Cobalt 10 ug/L I 10 OK MW-25 Coooer 10 ug/L u I 10 OK MW-25 Fluoride 0.1 mg/L I 0.1 OK MW-25 Gross Radium Alpha 0.763 oCi/L u 1 I OK MW-25 Iron 30 ug/L u I 30 OK MW-25 Lead I ug/L u I 1 OK MW-25 Magnesium 0.2 mg/L I 0.5 OK MW-25 Manganese 10 ug/L 1 10 OK MW-25 Mercury 0.5 ug/L u 1 0.5 OK MW-25 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-25 Methylene Chloride 1 ug/L u I I OK MW-25 Molybdenum 10 ug/L I 10 OK MW-25 Naphthalene I ug/L u I 1 OK MW-25 Nickel 20 ug/L u 1 20 OK MW-25 Nitrate + Nitrite as N 0.1 mg/L u I 0.1 OK MW-25 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-25 Potassium 0.5 mg/L 1 0.5 OK MW-25 Selenium 5 ug/L u 1 5 OK MW-25 Silver 10 ug/L u 1 10 OK MW-25 Sodium 0.5 mg/L I 0.5 OK MW-25 Sulfate 100 mg/L 100 I OK MW-25 Tetrahydrofuran I ug/L u 1 I OK G5AQ -I S I R uarter1y amp e eporung mut ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-25 Thallium 0.5 ug/L I 0.5 OK MW-25 Tin 100 ug/L u I 100 OK MW-25 Toluene I ug/L u I I OK MW-25 Total Dissolved Solids 20 MG/L 2 10 OK MW-25 Uranium 0.3 ug/L I 0.3 OK MW-25 Vanadium 15 ug/L u I 15 OK MW-25 Xylenes, total I ug/L u I I OK MW-25 Zinc 10 ug/L u I 10 OK MW-26 Acetone 20 ug/L u I 20 OK MW-26 Arsenic 5 ug/L u I 5 OK MW-26 Benzene I ug/L u I I OK MW-26 Beryllium 0.5 ug/L u I 0.5 OK MW-26 Bicarbonate as CaCO3 I mg/L I I OK MW-26 Cadmium 0.5 ug/L I 0.5 OK MW-26 Calcium 0.2 mg/L I 0.5 OK MW-26 Carbon Tetrachloride I ug/L u I 1 OK MW-26 Carbonate as CO3 1 mg/L u 1 1 OK MW-26 Chloride 1 mg/L 1 1 OK MW-26 Chloroform 100 ug/L 100 1 OK MW-26 Chloromethane I ug/L u I 1 OK MW-26 Chromium 25 ug/L u I 25 OK MW-26 Cobalt 10 ug/L u 1 10 OK MW-26 Copper 10 ug/L u 1 10 OK MW-26 Fluoride 0.1 mg/L 1 0.1 OK MW-26 Gross Radium Alpha 0.664 pCi/L 1 1 OK MW-26 Iron 30 ug/L 1 30 OK MW-26 Lead 1 ug/L u 1 1 OK MW-26 Magnesium 0.2 mg/L 1 0.5 OK MW-26 Manganese 10 ug/L 1 10 OK MW-26 Mercury 0.5 ug/L u 1 0.5 OK MW-26 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-26 Methylene Chloride 1 ug/L u 1 1 OK MW-26 Molybdenum 10 ug/L u 1 10 OK MW-26 Naphthalene 1 ug/L u 1 1 OK MW-26 Nickel 20 ug/L u 1 20 OK MW-26 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-26 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-26 Potassium 0.5 mg/L 1 0.5 OK MW-26 Selenium 5 ug/L 1 5 OK MW-26 Silver 10 ug/L u 1 10 OK MW-26 Sodium 0.5 mg/L 1 0.5 OK MW-26 Sulfate 100 mg/L 100 1 OK MW-26 Tetrahydrofuran 1 ug/L u 1 1 OK MW-26 Thallium 0.5 ug/L u 1 0.5 OK MW-26 Tin 100 ug/L u 1 100 OK MW-26 Toluene 1 ug/L u 1 1 OK MW-26 Total Dissolved Solids 20 MG/L 2 10 OK MW-26 Uranium 0.3 ug/L 1 0.3 OK MW-26 Vanadium 15 ug/L u 1 15 OK MW-26 Xylenes, total 1 ug/L u 1 1 OK MW-26 Zinc 10 ug/L u 1 10 OK MW-27 Acetone 20 ug/L u 1 20 OK MW-27 Arsenic 5 ug/L u 1 5 OK MW-27 Benzene 1 ug/L u 1 1 OK GSAQ -uarter y ampe eportmg I S IR mut ec L" . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-27 Beryllium 0.5 ug/L u I 0.5 OK MW-27 Bicarbonate as CaCO3 I mg/L I I OK MW-27 Cadmium 0.5 ug/L u 1 0.5 OK MW-27 Calcium 0.2 mg/L 1 0.5 OK MW-27 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-27 Carbonate as CO3 1 mg/L u 1 1 OK MW-27 Chloride 20 mg/L 20 1 OK MW-27 Chloroform I ug/L u 1 1 OK MW-27 Chloromethane 1 ug/L u 1 1 OK MW-27 Chromium 25 ug/L u I 25 OK MW-27 Cobalt 10 ug/L u I 10 OK MW-27 Copper 10 ug/L u 1 10 OK MW-27 Fluoride 0.2 mg/L 2 0.1 OK MW-27 Gross Radium Alpha 0.939 pCi/L u 1 1 OK MW-27 Iron 30 ug/L u 1 30 OK MW-27 Lead I ug/L u 1 1 OK MW-27 Magnesium 0.2 mg/L 1 0.5 OK MW-27 Manganese 10 ug/L u 1 10 OK MW-27 Mercury 0.5 ug/L u 1 0.5 OK MW-27 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-27 Methylene Chloride 1 ug/L u 1 1 OK MW-27 Molybdenum 10 ug/L u I 10 OK MW-27 Naphthalene 1 ug/L u I 1 OK MW-27 Nickel 20 ug/L u 1 20 OK MW-27 Nitrate + Nitrite as N 0.2 mg/L 2 0.1 OK MW-27 Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-27 Potassium 0.5 mg/L I 0.5 OK MW-27 Selenium 5 ug/L I 5 OK MW-27 Silver 10 ug/L u 1 10 OK MW-27 Sodium 0.5 mg/L 1 0.5 OK MW-27 Sulfate 20 mg/L 20 1 OK MW-27 Tetrahydrofuran 1 ug/L u 1 1 OK MW-27 Thallium 0.5 ug/L u I 0.5 OK MW-27 Tin 100 ug/L u 1 100 OK MW-27 Toluene 1 ug/L u 1 1 OK MW-27 Total Dissolved Solids 20 MG/L 2 10 OK MW-27 Uranium 0.3 ug/L 1 0.3 OK MW-27 Vanadium 15 ug/L u 1 15 OK MW-27 Xylenes, total 1 ug/L u I 1 OK MW-27 Zinc 10 ug/L u I 10 OK MW-28 Acetone 20 ug/L u I 20 OK MW-28 Arsenic 5 ug/L 1 5 OK MW-28 Benzene 1 ug/L u I 1 OK MW-28 Beryllium 0.5 ug/L u 1 0.5 OK MW-28 Bicarbonate as CaCO3 1 mg/L I 1 OK MW-28 Cadmium 0.5 ug/L I 0.5 OK MW-28 Calcium 0.2 mg/L I 0.5 OK MW-28 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-28 Carbonate as CO3 1 mg/L u 1 1 OK MW-28 Chloride 5 mg/L 5 1 OK MW-28 Chloroform 1 ug/L u 1 I OK MW-28 Chloromethane 1 ug/L u 1 1 OK MW-28 Chromium 25 ug/L u I 25 OK MW-28 Cobalt 10 ug/L 1 10 OK G5AQ -I S I R uarterty amp e eporllng mnt ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-28 Copper 10 ug/L u 1 10 OK MW-28 Fluoride 0.1 mg/L 1 0.1 OK MW-28 Gross Radium Alpha 0.606 pCi/L u 1 1 OK MW-28 Iron 30 ug/L u 1 30 OK MW-28 Lead 1 ug/L u 1 1 OK MW-28 Magnesium 0.2 mg/L 1 0.5 OK MW-28 Manganese 10 ug/L 1 10 OK MW-28 Mercury 0.5 ug/L u 1 0.5 OK MW-28 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-28 Methylene Chloride 1 ug/L u 1 1 OK MW-28 Molybdenum 10 ug/L u 1 10 OK MW-28 Naphthalene 1 ug/L u 1 I OK MW-28 Nickel 20 ug/L 1 20 OK MW-28 Nitrate + Nitrite as N 0.2 mg/L 2 0.1 OK MW-28 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-28 Potassium 0.5 mg/L 1 0.5 OK MW-28 Selenium 5 ug/L I 5 OK MW-28 Silver 10 ug/L u I 10 OK MW-28 Sodium 0.5 mg/L 1 0.5 OK MW-28 Sulfate 100 mg/L 100 1 OK MW-28 Tetrahydrofuran 1 ug/L u 1 1 OK MW-28 Thallium 0.5 ug/L 1 0.5 OK MW-28 Tin 100 ug/L u 1 100 OK MW-28 Toluene 1 ug/L u 1 I OK MW-28 Total Dissolved Solids 20 MG/L 2 10 OK MW-28 Uranium 0.3 ug/L 1 0.3 OK MW-28 Vanadium 15 ug/L u 1 15 OK MW-28 Xvlenes, total I ug/L u 1 1 OK MW-28 Zinc 10 ug/L 1 10 OK MW-29 Acetone 20 ug/L u 1 20 OK MW-29 Arsenic 5 ug/L 1 5 OK MW-29 Benzene I ug/L u 1 1 OK MW-29 Beryllium 0.5 ug/L u 1 0.5 OK MW-29 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-29 Cadmium 0.5 ug/L u 1 0.5 OK MW-29 Calcium 0.2 mg/L 1 0.5 OK MW-29 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-29 Carbonate as CO3 1 mg/L u 1 1 OK MW-29 Chloride 1 mg/L I 1 OK MW-29 Chloroform 1 ug/L u 1 1 OK MW-29 Chloromethane 1 ug/L u 1 1 OK MW-29 Chromium 25 ug/L u 1 25 OK MW-29 Cobalt 10 ug/L u 1 10 OK MW-29 Copper 10 ug/L u 1 10 OK MW-29 Fluoride 0.1 mg/L 1 0.1 OK MW-29 Gross Radium Alpha 0.754 pCi/L u 1 I OK MW-29 Iron 30 ug/L 1 30 OK MW-29 Lead I ug/L u I I OK MW-29 Magnesium 0.2 mg/L I 0.5 OK MW-29 Manganese 10 ug/L 10 10 OK MW-29 Mercury 0.5 ug/L u 1 0.5 OK MW-29 Methyl Ethyl Ketone 20 ug/L u I 20 OK MW-29 Methylene Chloride 1 ug/L u I 1 OK MW-29 Molybdenum 10 ug/L u I 10 OK G5AQ -l S I R uarterty amp. e eporLmg urut ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-29 Naphthalene I ug/L u I 1 OK MW-29 Nickel 20 ug/L u 1 20 OK MW-29 Nitrate + Nitrite as N 0.1 mg/L u 1 0.1 OK MW-29 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-29 Potassium 0.5 mg/L 1 0.5 OK MW-29 Selenium 5 ug/L u I 5 OK MW-29 Silver IO ug/L u 1 IO OK MW-29 Sodium 0.5 mg/L I 0.5 OK MW-29 Sulfate 100 mg/L 100 1 OK MW-29 Tetrahydrofuran I ug/L u I 1 OK MW-29 Thallium 0.5 ug/L u I 0.5 OK MW-29 Tin 100 ug/L u 1 100 OK MW-29 Toluene I ug/L u I I OK MW-29 Total Dissolved Solids 20 MG/L 2 IO OK MW-29 Uranium 0.3 ug/L 1 0.3 OK MW-29 Vanadium 15 ug/L u 1 15 OK MW-29 Xylenes, total 1 ug/L u 1 1 OK MW-29 Zinc IO ug/L u 1 IO OK MW-30 Acetone 20 ug/L u 1 20 OK MW-30 Arsenic 5 ug/L u I 5 OK MW-30 Benzene 1 ug/L u I 1 OK MW-30 Beryllium 0.5 ug/L u 1 0.5 OK MW-30 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-30 Cadmium 0.5 ug/L u 1 0.5 OK MW-30 Calcium 0.2 mg/L 1 0.5 OK MW-30 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-30 Carbonate as CO3 1 mg/L u I I OK MW-30 Chloride 5 mg/L 5 1 OK MW-30 Chloroform 1 ug/L u 1 1 OK MW-30 Chloromethane 1 ug/L u 1 1 OK MW-30 Chromium 25 ug/L u 1 25 OK MW-30 Cobalt IO ug/L u I IO OK MW-30 Copper IO ug/L u I IO OK MW-30 Fluoride 0.1 mg/L I 0.1 OK MW-30 Gross Radium Alpha 0.746 pCi/L u I 1 OK MW-30 Iron 30 ug/L u 1 30 OK MW-30 Lead I ug/L u I I OK MW-30 Magnesium 0.2 mg/L 1 0.5 OK MW-30 Manganese IO ug/L u 1 IO OK MW-30 Mercury 0.5 ug/L u 1 0.5 OK MW-30 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-30 Methylene Chloride 1 ug/L u I 1 OK MW-30 Molybdenum IO ug/L u I IO OK MW-30 Naphthalene 1 ug/L u I I OK MW-30 Nickel 20 ug/L u I 20 OK MW-30 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-30 Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-30 Potassium 0.5 mg/L I 0.5 OK MW-30 Selenium 5 ug/L I 5 OK MW-30 Silver 10 ug/L u I 10 OK MW-30 Sodium 0.5 mg/L I 0.5 OK MW-30 Sulfate 100 mg/L 100 1 OK MW-30 Tetrahydrofuran 1 ug/L u 1 1 OK MW-30 Thallium 0.5 ug/L u I 0.5 OK G5AQ -uarter y ampe epor I S 1 R ng umt ec Ii L" . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-30 Tin 100 ug/L u I 100 OK MW-30 Toluene 1 ug/L u 1 1 OK MW-30 Total Dissolved Solids 20 MG/L 2 10 OK MW-30 Uranium 0.3 ug/L I 0.3 OK MW-30 Vanadium 15 ug/L u 1 15 OK MW-30 Xylenes, total 1 ug/L u 1 1 OK MW-30 Zinc 10 ug/L u 1 10 OK MW-31 Acetone 20 ug/L u 1 20 OK MW-31 Arsenic 5 ug/L u 1 5 OK MW-31 Benzene 1 ug/L u 1 1 OK MW-31 Beryllium 0.5 ug/L u 1 0.5 OK MW-31 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-31 Cadmium 0.5 ug/L u 1 0.5 OK MW-31 Calcium 0.2 mg/L 1 0.5 OK MW-31 Carbon Tetrachloride I ug/L u 1 1 OK MW-31 Carbonate as CO3 1 mg/L u 1 1 OK MW-31 Chloride 10 mg/L 10 1 OK MW-31 Chloroform 1 ug/L u 1 1 OK MW-31 Chloromethane 1 ug/L u 1 1 OK MW-31 Chromium 25 ug/L u 1 25 OK MW-31 Cobalt 10 ug/L u 1 IO OK MW-31 Copper 10 ug/L u I 10 OK MW-31 Fluoride 0.1 mg/L 1 0.1 OK MW-31 Gross Radium Alpha 0.795 pCi/L 1 1 OK MW-31 Iron 30 ug/L u I 30 OK MW-31 Lead 1 ug/L u 1 1 OK MW-31 Magnesium 0.2 mg/L 1 0.5 OK MW-31 Manganese 10 ug/L u 1 10 OK MW-31 Mercury 0.5 ug/L u I 0.5 OK MW-31 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-31 Methylene Chloride 1 ug/L u 1 1 OK MW-31 Molybdenum 10 ug/L u 1 IO OK MW-31 Naphthalene 1 ug/L u 1 I OK MW-31 Nickel 20 ug/L u 1 20 OK MW-31 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-31 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-31 Potassium 0.5 mg/L 1 0.5 OK MW-31 Selenium 5 ug/L 1 5 OK MW-31 Silver 10 ug/L u 1 10 OK MW-31 Sodium 0.5 mg/L 1 0.5 OK MW-31 Sulfate 100 mg/L 100 I OK MW-31 Tetrahydrofuran 1 ug/L u 1 1 OK MW-31 Thallium 0.5 ug/L u 1 0.5 OK MW-31 Tin 100 ug/L u 1 100 OK MW-31 Toluene 1 ug/L u 1 1 OK MW-31 Total Dissolved Solids 20 MG/L 2 10 OK MW-31 Uranium 0.3 ug/L 1 0.3 OK MW-31 Vanadium 15 ug/L u 1 15 OK MW-31 Xvlenes, total 1 ug/L u I I OK MW-31 Zinc 10 ug/L u 1 IO OK MW-32 Acetone 20 ug/L u 1 20 OK MW-32 Arsenic 5 ug/L u 1 5 OK MW-32 Benzene 1 ug/L u 1 1 OK MW-32 Beryllium 0.5 ug/L u I 0.5 OK G5AQ -I S I R uarter1y amp e eporting nrut ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-32 Bicarbonate as CaCO3 1 mg/L 1 I OK MW-32 Cadmium 0.5 ug/L I 0.5 OK MW-32 Calcium 0.2 mg/L I 0.5 OK MW-32 Carbon Tetrachloride I ug/L u 1 I OK MW-32 Carbonate as CO3 1 mg/L u 1 1 OK MW-32 Chloride 1 mg/L 1 1 OK MW-32 Chloroform 1 ug/L u 1 1 OK MW-32 Chloromethane 1 ug/L u 1 1 OK MW-32 Chromium 25 ug/L u 1 25 OK MW-32 Cobalt 10 ug/L 1 10 OK MW-32 Copper 10 ug/L u 1 10 OK MW-32 Fluoride 0.1 mg/L 1 0.1 OK MW-32 Iron 30 ug/L 1 30 OK MW-32 Lead 1 ug/L u 1 1 OK MW-32 Magnesium 0.2 mg/L 1 0.5 OK MW-32 Manganese 10 ug/L 10 10 OK MW-32 Mercury 0.5 ug/L u 1 0.5 OK MW-32 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-32 Methylene Chloride I ug/L u 1 1 OK MW-32 Molybdenum 10 ug/L 1 10 OK MW-32 Naphthalene 1 ug/L u 1 1 OK MW-32 Nickel 20 ug/L 1 20 OK MW-32 Nitrate + Nitrite as N 0.1 mg/L u 1 0.1 OK MW-32 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-32 Potassium 0.5 mg/L 1 0.5 OK MW-32 Selenium 5 ug/L u 1 5 OK MW-32 Silver 10 ug/L u 1 10 OK MW-32 Sodium 0.5 mg/L 1 0.5 OK MW-32 Sulfate 100 mg/L 100 1 OK MW-32 Tetrahydrofuran 1 ug/L u 1 1 OK MW-32 Thallium 0.5 ug/L u 1 0.5 OK MW-32 Tin 100 ug/L u I 100 OK MW-32 Toluene 1 ug/L u 1 1 OK MW-32 Total Dissolved Solids 20 MG/L 2 10 OK MW-32 Uranium 0.3 ug/L 1 0.3 OK MW-32 Vanadium 15 ug/L u 1 15 OK MW-32 Xylenes, total 1 ug/L u 1 1 OK MW-32 Zinc 10 ug/L 1 10 OK MW-32 Gross Radium Alpha 0.933 pCi/L 1 1 OK MW-35 Acetone 20 ug/L u 1 20 OK MW-35 Arsenic -5 ug/L u 1 5 OK MW-35 Benzene 1 ug/L u 1 1 OK MW-35 Beryllium 0.5 ug/L u 1 0.5 OK MW-35 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-35 Cadmium 0.5 ug/L u 1 0.5 OK MW-35 Calcium 0.2 mg/L 1 0.5 OK MW-35 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-35 Carbonate as CO3 1 mg/L u 1 1 OK MW-35 Chloride 1 mg/L 1 1 OK MW-35 Chloroform 1 ug/L u 1 1 OK MW-35 Chloromethane 1 ug/L u 1 1 OK MW-35 Chromium 25 ug/L u 1 25 OK MW-35 Cobalt 10 ug/L u 1 10 OK MW-35 Coooer 10 ug/L u 1 10 OK G5AQ -I S l R uarterly amp e eporung urut ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-35 Fluoride 0.1 mg/L 1 0.1 OK MW-35 Gross Radium Alpha 0.819 oCi/L 1 1 OK MW-35 Iron 30 ug/L 1 30 OK MW-35 Lead 1 ug/L u 1 1 OK MW-35 Magnesium 0.2 mg/L 1 0.5 OK MW-35 Manganese 10 ug/L 1 10 OK MW-35 Mercury 0.5 ug/L u 1 0.5 OK MW-35 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-35 Methylene Chloride 1 ug/L u 1 1 OK MW-35 Molybdenum 10 ug/L u 1 10 OK MW-35 Naphthalene 1 ug/L u 1 1 OK MW-35 Nickel 20 ug/L u 1 20 OK MW-35 Nitrate + Nitrite as N 0.1 mg/L u 1 0.1 OK MW-35 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-35 Potassium 0.5 mg/L 1 0.5 OK MW-35 Selenium 5 ug/L 1 5 OK MW-35 Silver 10 ug/L u 1 10 OK MW-35 Sodium 0.5 mg/L 1 0.5 OK MW-35 Sulfate 50 mg/L 50 1 OK MW-35 Tetrahydrofuran 1 ug/L u 1 1 OK MW-35 Thallium 0.5 ug/L u 1 0.5 OK MW-35 Tin 100 ug/L u 1 100 OK MW-35 Toluene 1 ug/L u 1 1 OK MW-35 Total Dissolved Solids 20 MG/L 2 10 OK MW-35 Uranium 0.3 ug/L 1 0.3 OK MW-35 Vanadium 15 ug/L u 1 15 OK MW-35 Xylenes, total 1 ug/L u 1 1 OK MW-35 Zinc 10 ug/L u 1 10 OK MW-36 Acetone 20 ug/L u 1 20 OK MW-36 Arsenic 5 ug/L u 1 5 OK MW-36 Benzene 1 ug/L u 1 1 OK MW-36 Beryllium 0.5 ug/L u 1 0.5 OK MW-36 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-36 Cadmium 0.5 ug/L u 1 0.5 OK MW-36 Calcium 0.2 mg/L 1 0.5 OK MW-36 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-36 Carbonate as CO3 1 mg/L u 1 1 OK MW-36 Chloride 1 mg/L 1 1 OK MW-36 Chloroform 1 ug/L u 1 1 OK MW-36 Chloromethane 1 ug/L u 1 1 OK MW-36 Chromium 25 ug/L u 1 25 OK MW-36 Cobalt 10 ug/L u 1 10 OK MW-36 Cooner 10 ug/L u 1 10 OK MW-36 Fluoride 0.1 mg/L 1 0.1 OK MW-36 Gross Radium Alpha 0.723 pCi/L 1 1 OK MW-36 Iron 30 ug/L u 1 30 OK MW-36 Lead 1 ug/L u 1 1 OK MW-36 Magnesium 0.2 mg/L 1 0.5 OK MW-36 Manganese 10 ug/L u 1 10 OK MW-36 Mercury 0.5 ug/L u 1 0.5 OK MW-36 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-36 Methylene Chloride I ug/L u I 1 OK MW-36 Molybdenum 10 ug/L u I 10 OK MW-36 Naphthalene I ug/L u 1 I OK G5AQ -I S IR uarteriy amp e eportmg nmt ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-36 Nickel 20 ug/L u 1 20 OK MW-36 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-36 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-36 Potassium 0.5 mg/L 1 0.5 OK MW-36 Selenium 5 ug/L 1 5 OK MW-36 Silver 10 ug/L u 1 10 OK MW-36 Sodium 5 mg/L 10 0.5 OK MW-36 Sulfate 100 mg/L 100 1 OK MW-36 Tetrahydrofuran 1 ug/L u 1 1 OK MW-36 Thallium 0.5 ug/L 1 0.5 OK MW-36 Tin 100 ug/L u 1 100 OK MW-36 Toluene 1 ug/L u 1 1 OK MW-36 Total Dissolved Solids 20 MG/L 2 10 OK MW-36 Uranium 0.3 ug/L 1 0.3 OK MW-36 Vanadium 15 ug/L u 1 15 OK MW-36 Xylenes, total 1 ug/L u 1 1 OK MW-36 Zinc 10 ug/L u 1 10 OK MW-37 Acetone 20 ug/L u 1 20 OK MW-37 Arsenic 5 ug/L u 1 5 OK MW-37 Benzene 1 ug/L u 1 1 OK MW-37 Beryllium 0.5 ug/L u 1 0.5 OK MW-37 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-37 Cadmium 0.5 ug/L u 1 0.5 OK MW-37 Calcium 0.2 mg/L 1 0.5 OK MW-37 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-37 Carbonate as CO3 1 mg/L u 1 1 OK MW-37 Chloride 1 mg/L 1 1 OK MW-37 Chloroform 1 ug/L u 1 1 OK MW-37 Chloromethane 1 ug/L u 1 1 OK MW-37 Chromium 25 ug/L u 1 25 OK MW-37 Cobalt 10 ug/L u 1 10 OK MW-37 Coover 10 ug/L u 1 10 OK MW-37 Fluoride 0.1 mg/L 1 0.1 OK MW-37 Gross Radium Alpha 0.659 pCi/L u 1 1 OK MW-37 Iron 30 ug/L u 1 30 OK MW-37 Lead 1 ug/L u 1 1 OK MW-37 Magnesium 0.2 mg/L 1 0.5 OK MW-37 Manganese 10 ug/L 1 10 OK MW-37 Mercury 0.5 ug/L u 1 0.5 OK MW-37 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-37 Methylene Chloride 1 ug/L u 1 1 OK MW-37 Molybdenum 10 ug/L u 1 10 OK MW-37 Naphthalene 1 ug/L u 1 1 OK MW-37 Nickel 20 ug/L u 1 20 OK MW-37 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-37 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-37 Potassium 0.5 mg/L 1 0.5 OK MW-37 Selenium 5 u11;/L 1 5 OK MW-37 Silver 10 ug/L u 1 10 OK MW-37 Sodium 0.5 mg/L 1 0.5 OK MW-37 Sulfate 50 mg/L 50 1 OK MW-37 Tetrahydrofuran 1 ug/L u 1 1 OK MW-37 Thallium 0.5 ug/L 1 0.5 OK MW-37 Tin 100 ug/L u 1 100 OK G5AQ -I S I R uarter y amp e eportmg umt ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-37 Toluene 1 ug/L u 1 I OK MW-37 Total Dissolved Solids 20 MG/L 2 IO OK MW-37 Uranium 0.3 ug/L 1 0.3 OK MW-37 Vanadium 15 ug/L u 1 15 OK MW-37 Xylenes, total I ug/L u I 1 OK MW-37 Zinc IO ug/L 1 10 OK MW-38 Acetone 20 ug/L u 1 20 OK MW-38 Arsenic 5 ug/L u 1 5 OK MW-38 Benzene 1 ug/L u 1 1 OK MW-38 Beryllium 0.5 ug/L u 1 0.5 OK MW-38 Bicarbonate as CaCO3 1 mg/L 1 I OK MW-38 Cadmium 0.5 ug/L u I 0.5 OK MW-38 Calcium 0.2 mg/L 1 0.5 OK MW-38 Carbon Tetrachloride 1 ug/L u I 1 OK MW-38 Carbonate as CO3 1 mg/L u 1 1 OK MW-38 Chloride 1 mg/L 1 1 OK MW-38 Chloroform 1 ug/L u 1 1 OK MW-38 Chloromethane 1 ug/L u 1 1 OK MW-38 Chromium 25 ug/L u 1 25 OK MW-38 Cobalt 10 ug/L u 1 10 OK MW-38 Copper 10 ug/L u 1 10 OK MW-38 Fluoride 0.1 mg/L 1 0.1 OK MW-38 Gross Radium Alpha 0.566 pCi/L u 1 I OK MW-38 Iron 30 ug/L u I 30 OK MW-38 Lead I ug/L u 1 1 OK MW-38 Magnesium 0.2 mg/L I 0.5 OK MW-38 Manganese 10 ug/L u 1 10 OK MW-38 Mercury 0.5 ug/L u 1 0.5 OK MW-38 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-38 Methylene Chloride 1 ug/L u 1 1 OK MW-38 Molybdenum 10 ug/L u I 10 OK MW-38 Naphthalene 1 ug/L u 1 1 OK MW-38 Nickel 20 ug/L u 1 20 OK MW-38 Nitrate + Nitrite as N 4.8 mg/L 48 0.1 OK MW-38 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-38 Potassium 0.5 mg/L 1 0.5 OK MW-38 Selenium 5 ug/L 1 5 OK MW-38 Silver 10 ug/L u 1 10 OK MW-38 Sodium 0.5 mg/L 1 0.5 OK MW-38 Sulfate 50 mg/L 50 1 OK MW-38 Tetrahydrofuran 1 ug/L u 1 1 OK MW-38 Thallium 0.5 ug/L u 1 0.5 OK MW-38 Tin 100 ug/L u 1 100 OK MW-38 Toluene 1 ug/L u 1 1 OK MW-38 Total Dissolved Solids 20 MG/L 2 10 OK MW-38 Uranium 0.3 ug/L 1 0.3 OK MW-38 Vanadium 15 ug/L u 1 15 OK MW-38 Xylenes, total 1 ug/L u 1 1 OK MW-38 Zinc IO ug/L u 1 IO OK MW-39 Acetone 20 ug/L u 1 20 OK MW-39 Arsenic 5 ug/L u 1 5 OK MW-39 Benzene 1 ug/L u I 1 OK MW-39 Beryllium 0.5 ug/L 1 0.5 OK MW-39 Bicarbonate as CaCO3 1 mg/L u 1 1 OK G5AQ -I S I R uarcer1y amp e eportmg 1m1t ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-39 Cadmium 0.5 ug/L 1 0.5 OK MW-39 Calcium 0.2 mg/L 1 0.5 OK MW-39 Carbon Tetrachloride I ug/L u I 1 OK MW-39 Carbonate as CO3 I mg/L u I I OK MW-39 Chloride 20 mg/L 20 I OK MW-39 Chloroform I ug/L u I I OK MW-39 Chloromethane 1 ug/L u I I OK MW-39 Chromium 25 uwl, u 1 25 OK MW-39 Cobalt 10 ug/L I 10 OK MW-39 Copper 10 ug/L I 10 OK MW-39 Fluoride 0.2 mg/L 2 0.1 OK MW-39 Iron 30 uwl, I 30 OK MW-39 Lead 1 ug/L u I 1 OK MW-39 Magnesium 0.2 mg/L 1 0.5 OK MW-39 Manganese 10 ug/L 1 10 OK MW-39 Mercury 0.5 uwl, u 1 0.5 OK MW-39 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-39 Methylene Chloride 1 ug/L u 1 1 OK MW-39 Molybdenum 10 ug/L u 1 10 OK MW-39 Naphthalene 1 ug/L u 1 1 OK MW-39 Nickel 20 ug/L 1 20 OK MW-39 Nitrate + Nitrite as N 0.1 mg/L u 1 0.1 OK MW-39 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-39 Potassium 0.5 mg/L 1 0.5 OK MW-39 Selenium 5 ug/L 1 5 OK MW-39 Silver 10 ug/L u 1 10 OK MW-39 Sodium 5 mg/L 10 0.5 OK MW-39 Sulfate 50 mg/L 50 1 OK MW-39 Tetrahydrofuran 1 ug/L u 1 1 OK MW-39 Thallium 0.5 ug/L 1 0.5 OK MW-39 Tin 100 ug/L u 1 100 OK MW-39 Toluene 1 ug/L u 1 1 OK MW-39 Total Dissolved Solids 20 MG/L 2 10 OK MW-39 Uranium 0.3 ug/L 1 0.3 OK MW-39 Vanadium 15 ug/L u 1 15 OK MW-39 Xylenes, total 1 ug/L u 1 1 OK MW-39 Zinc 10 ug/L 1 10 OK MW-39 Gross Radium Alpha 0.787 pCi/L 1 1 OK MW-40 Acetone 20 ug/L u 1 20 OK MW-40 Arsenic 5 ug/L u 1 5 OK MW-40 Benzene 1 ug/L u 1 1 OK MW-40 Beryllium 0.5 ug/L u I 0.5 OK MW-40 Bicarbonate as CaCO3 I mg/L 1 1 OK MW-40 Cadmium 0.5 ug/L u 1 0.5 OK MW-40 Calcium 0.2 mg/L 1 0.5 OK MW-40 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-40 Carbonate as CO3 1 mg/L u 1 I OK MW-40 Chloride 20 mg/L 20 1 OK MW-40 Chloroform 1 ug/L u 1 1 OK MW-40 Chloromethane 1 ug/L u 1 1 OK MW-40 Chromium 25 ug/L u 1 25 OK MW-40 Cobalt 10 ug/L u 1 10 OK MW-40 Copper 10 ug/L u 1 10 OK MW-40 Fluoride 0.2 mg/L 2 0.1 OK GSAQ -I S I R uartenv amp e eportmg urut ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-40 Gross Radium Alpha 0.622 pCi/L 1 1 OK MW-40 Iron 30 ug/L u 1 30 OK MW-40 Lead 1 ug/L u 1 1 OK MW-40 Magnesium 0.2 mg/L 1 0.5 OK MW-40 Manganese 10 ug/L 1 10 OK MW-40 Mercury 0.5 ug/L u 1 0.5 OK MW-40 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-40 Methylene Chloride 1 ug/L u 1 1 OK MW-40 Molybdenum 10 ug/L u 1 10 OK MW-40 Naphthalene 1 ug/L u 1 1 OK MW-40 Nickel 20 ug/L u 1 20 OK MW-40 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-40 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-40 Potassium 0.5 mg/L 1 0.5 OK MW-40 Selenium 5 ug/L 1 5 OK MW-40 Silver 10 ug/L u 1 10 OK MW-40 Sodium 0.5 mg/L 1 0.5 OK MW-40 Sulfate 20 mg/L 20 I OK MW-40 Tetrahydrofuran 1 ug/L u 1 I OK MW-40 Thallium 0.5 ug/L u 1 0.5 OK MW-40 Tin 100 ug/L u 1 100 OK MW-40 Toluene 1 ug/L u 1 I OK MW-40 Total Dissolved Solids 20 MG/L 2 10 OK MW-40 Uranium 0.3 ug/L 1 0.3 OK MW-40 Vanadium 15 ug/L u I 15 OK MW-40 Xylenes, total 1 ug/L u 1 1 OK MW-40 Zinc 10 ug/L u 1 10 OK MW-12 Acetone 20 ug/L u 1 20 OK MW-12 Arsenic 5 ug/L u 1 5 OK MW-12 Benzene 1 ug/L u 1 1 OK MW-12 Beryllium 0.5 ug/L u I 0.5 OK MW-12 Bicarbonate as CaCO3 1 mg/L I 1 OK MW-12 Cadmium 0.5 ug/L u 1 0.5 OK MW-12 Calcium 0.2 mg/L 1 0.5 OK MW-12 Carbon Tetrachloride 1 ug/L u 1 1 OK MW-12 Carbonate as CO3 1 mg/L u 1 1 OK MW-65 Chloride 1 mg/L 1 1 OK MW-65 Chloroform 1 ug/L u 1 1 OK MW-65 Chloromethane 1 ug/L u 1 I OK MW-65 Chromium 25 ug/L u 1 25 OK MW-65 Cobalt 10 ug/L u 1 10 OK MW-65 Copper 10 ug/L u 1 10 OK MW-65 Fluoride 0.1 mg/L u I 0.1 OK MW-65 Gross Radium Alpha 0.809 pCi/L u I 1 OK MW-65 Iron 30 ug/L u I 30 OK MW-65 Lead I ug/L u 1 1 OK MW-65 Magnesium 0.2 mg/L 1 0.5 OK MW-65 Manganese 10 ug/L 1 10 OK MW-65 Mercury 0.5 ug/L u I 0.5 OK MW-65 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-65 Methylene Chloride 1 ug/L u 1 1 OK MW-65 Molybdenum 10 ug/L u 1 10 OK MW-65 Naphthalene 1 ug/L u I 1 OK MW-65 Nickel 20 ug/L u 1 20 OK G5AQ -I S I R uarter1y amp e eporttng umt ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-65 Nitrate + Nitrite as N 0.1 mg/L I 0.1 OK MW-65 Nitrogen, Ammonia as N 0.05 mg/L I 0.05 OK MW-65 Potassium 0.5 mg/L I 0.5 OK MW-65 Selenium 5 ug/L I 5 OK MW-65 Silver IO ug/L u I 10 OK MW-65 Sodium 0.5 mg/L I 0.5 OK MW-65 Sulfate 100 mg/L 100 I OK MW-65 Tetrahydrofuran I ug/L u I I OK MW-65 Thallium 0.5 ug/L u I 0.5 OK MW-65 Tin 100 ug/L u I 100 OK MW-65 Toluene I ug/L u I I OK MW-65 Total Dissolved Solids 20 MG/L 2 IO OK MW-65 Uranium 0.3 ug/L I 0.3 OK MW-65 Vanadium 15 ug/L u I 15 OK MW-65 Xylenes, total I ug/L u I I OK MW-65 Zinc IO ug/L u 1 IO OK MW-70 Acetone 20 ug/L u 1 20 OK MW-70 Arsenic 5 ug/L u 1 5 OK MW-70 Benzene I ug/L u I I OK MW-70 Beryllium 0.5 ug/L u I 0.5 OK MW-70 Bicarbonate as CaCO3 I mg/L I I OK MW-70 Cadmium 0.5 ug/L u I 0.5 OK MW-70 Calcium 0.2 mg/L I 0.5 OK MW-70 Carbon Tetrachloride I ug/L u I I OK MW-70 Carbonate as CO3 1 mg/L u I 1 OK MW-70 Chloride I mg/L I 1 OK MW-70 Chloroform I ug/L u I I OK MW-70 Chloromethane I ug/L u I 1 OK MW-70 Chromium 25 ug/L u 1 25 OK MW-70 Cobalt IO ug/L u I 10 OK MW-70 Copper 10 ug/L u 1 10 OK MW-70 Fluoride 0.1 mg/L I 0.1 OK MW-70 Gross Radium Alpha 0.721 pCi/L I I OK MW-70 Iron 30 ug/L I 30 OK MW-70 Lead I ug/L u I 1 OK MW-70 Magnesium 0.2 mg/L I 0.5 OK MW-70 Manganese 10 ug/L I 10 OK MW-70 Mercury 0.5 ug/L u I 0.5 OK MW-70 Methyl Ethyl Ketone 20 ug/L u 1 20 OK MW-70 Methylene Chloride I ug/L u I I OK MW-70 Molybdenum IO ug/L u I 10 OK MW-70 Naphthalene I ug/L u I I OK MW-70 Nickel 20 ug/L u I 20 OK MW-70 Nitrate + Nitrite as N 0.1 mg/L u I 0.1 OK MW-70 Nitrogen, Ammonia as N 0.05 mg/L u I 0.05 OK MW-70 Potassium 0.5 mg/L 1 0.5 OK MW-70 Selenium 5 ug/L 1 5 OK MW-70 Silver 10 ug/L u I IO OK MW-70 Sodium 0.5 mg/L 1 0.5 OK MW-70 Sulfate 50 mg/L 50 I OK MW-70 Tetrahydrofuran I ug/L u 1 I OK MW-70 Thallium 0.5 ug/L u I 0.5 OK MW-70 Tin 100 ug/L u I 100 OK MW-70 Toluene 1 ug/L u I I OK G5AQ -uarteny amp.e I S J R eportmg 11111t ec L" . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-70 Total Dissolved Solids 20 MG/L 2 10 OK MW-70 Uranium 0.3 ug/L 1 0.3 OK MW-70 Vanadium 15 ug/L u 1 15 OK MW-70 Xylenes, total 1 ug/L u 1 1 OK MW-70 Zinc 10 ug/L u 1 10 OK TW4-24 Acetone 20 ug/L u 1 20 OK TW4-24 Arsenic 5 ug/L 1 5 OK TW4-24 Benzene 1 ug/L u 1 1 OK TW4-24 Beryllium 0.5 ug/L u 1 0.5 OK TW4-24 Bicarbonate as CaCO3 1 mg/L 1 1 OK TW4-24 Cadmium 0.5 ug/L 1 0.5 OK TW4-24 Calcium 0.2 mg/L 1 0.5 OK TW4-24 Carbon Tetrachloride 1 ug/L u 1 1 OK TW4-24 Carbonate as CO3 1 mg/L u 1 1 OK TW4-24 Chloride 50 mg/L 50 1 OK TW4-24 Chloroform 10 ug/L 10 1 OK TW4-24 Chloromethane 1 ug/L u 1 1 OK TW4-24 Chromium 25 ug/L u 1 25 OK TW4-24 Cobalt 10 ug/L u 1 10 OK TW4-24 Copper 10 ug/L u 1 10 OK TW4-24 Fluoride 0.1 mg/L 1 0.1 OK TW4-24 Gross Radium Alpha 0.634 pCi/L u 1 1 OK TW4-24 Iron 30 ug/L u 1 30 OK TW4-24 Lead 1 ug/L u 1 1 OK TW4-24 Magnesium 0.2 mg/L 1 0.5 OK TW4-24 Manganese 10 ug/L 1 10 OK TW4-24 Mercury 0.5 ug/L u 1 0.5 OK TW4-24 Methyl Ethyl Ketone 20 ug/L u 1 20 OK TW4-24 Methylene Chloride 1 ug/L u 1 1 OK TW4-24 Molybdenum 10 ug/L 1 10 OK TW4-24 Naphthalene 1 ug/L u 1 1 OK TW4-24 Nickel 20 ug/L 1 20 OK TW4-24 Nitrate + Nitrite as N 1 mg/L 10 0.1 OK TW4-24 Nitrogen, Ammonia as N 0.5 mg/L 10 0.05 OK TW4-24 Potassium 0.5 mg/L 1 0.5 OK TW4-24 Selenium 5 ug/L 1 5 OK TW4-24 Silver 10 ug/L u 1 10 OK TW4-24 Sodium 5 mg/L 10 0.5 OK TW4-24 Sulfate 50 mg/L 50 1 OK TW4-24 Tetrahydrofuran 1 ug/L 1 1 OK TW4-24 Thallium 0.5 ug/L 1 0.5 OK TW4-24 Tin 100 ug/L u 1 100 OK TW4-24 Toluene 1 ug/L u 1 1 OK TW4-24 Total Dissolved Solids 20 MG/L 2 10 OK TW4-24 Uranium 0.3 ug/L 1 0.3 OK TW4-24 Vanadium 15 ug/L u 1 15 OK TW4-24 Xylenes, total 1 ug/L u 1 1 OK TW4-24 Zinc 10 ug/L u 1 10 OK G5BA -cce erate dS IR amp e eporung mnt ec L" . Ch k Lab Required Reporting Dilution Reporting Location Analyte Limit Units Qualifier Factor Limit RLCheck Trip Blank Chloroform 1 ug/L u 1 1 OK Trip Blank Chloroform 1 ug/L u 1 1 OK MW-11 Sulfate 50 mg/L 50 1 OK MW-11 Chloride 1 mg/L 1 1 OK MW-11 Manganese 10 ug/L 1 10 OK MW-11 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-11 Total Dissolved Solids 20 MG/L 2 10 OK MW-11 Sulfate 20 mg/L 20 I OK MW-11 Chloride I mg/L I I OK MW-11 Manganese 10 ug/L I 10 OK MW-11 Nitrate + Nitrite as N 0.1 mp;/L 1 0.1 OK MW-11 Total Dissolved Solids 20 MG/L 2 10 OK MW-25 Total Dissolved Solids 20 MG/L 2 10 OK MW-25 Total Dissolved Solids 20 MG/L 2 10 OK MW-26 Chloride I mg/L I I OK MW-26 Chloroform 50 ug/L 50 1 OK MW-26 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-26 Chloride I mg/L 1 1 OK MW-26 Chloroform 100 up;/L 100 I OK MW-26 Nitrate + Nitrite as N 0.1 mg/L 1 0.1 OK MW-30 Chloride 5 mg/L 5 1 OK MW-30 Uranium 0.3 up;/L 1 0.3 OK MW-30 Selenium 5 ug/L I 5 OK MW-30 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-30 Chloride 5 mg/L 5 I OK MW-30 Uranium 0.3 up;/L I 0.3 OK MW-30 Selenium 5 ug/L I 5 OK MW-30 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-31 Sulfate 20 mg/L 20 I OK MW-31 Chloride 5 mg/L 5 1 OK MW-31 Uranium 0.3 ug/L 1 0.3 OK MW-31 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-31 Total Dissolved Solids 20 MG/L 2 10 OK MW-31 Sulfate 20 mg/L 20 1 OK MW-31 Chloride 5 mg/L 5 I OK MW-31 Uranium 0.3 ug/L 1 0.3 OK MW-31 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-31 Total Dissolved Solids 20 MG/L 2 10 OK MW-65 Chloride 5 mg/L 5 1 OK MW-65 Uranium 0.3 ug/L 1 0.3 OK MW-65 Selenium 5 ug/L 1 5 OK MW-65 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK MW-65 Chloride 5 mg/L 5 1 OK MW-65 Uranium 0.3 ug/L 1 0.3 OK MW-65 Selenium 5 ug/L 1 5 OK MW-65 Nitrate + Nitrite as N 0.5 mg/L 5 0.1 OK G-6A: Quarterly Sample Trip Blank Evaluation Lab Report Constituent Result 2-Butanone ND Acetone ND Benzene ND Carbon Tetrachloride ND Chloroform ND CTF 2211153 Chloromethane ND Methylene Chloride ND Naphthalene ND Tetrahydrofuran ND Toluene ND Xylenes, Total ND 2-Butanone ND Acetone ND Benzene ND Carbon Tetrachloride ND Chloroform ND CTF 2211703 Chloromethane ND Methylene Chloride ND Naphthalene ND Tetrahydrofuran ND Toluene ND Xylenes, Total ND 2-Butanone ND Acetone ND Benzene ND Carbon Tetrachloride ND Chloroform ND CTF22K0334 Chloromethane ND ND Naphthalene ND Tetrahydrofuran ND Toluene ND Xylenes, Total ND G-6B: Accelerated Sample Trip Blank Evaluation All trip blanks for the Accelerated samples were non detect. Blank Sample Date Laboratory CTF 22K0963 -November 11/10/2022 CTF CTF 22L1318 -December 12/15/2022 CTF G-7A: QA/QC Q Eva uation for . uarterly Sample D uplicates Constituent MW-12 MW-65 %RPO 10/13/22 10/13/22 Ammonia (as N) (mg/L) <0.0500 0.620 NIA Bicarbonate as CaCO3 (mg/L) 343 344 0.29 Calcium (mg/L) 513 509 0.78 Chloride (mg/L) 67.0 67.0 0.00 Fluoride (mg/L) 0.130 <0.100 NIA Magnesium (mg/L) 228 226 0.88 Manganese (mg/L) 0.0106 0.0106 0.00 Nitrate + Nitrite (as N) (mg/L) 0.149 0.137 8.39 Potassium (mg/L) 13.5 13.4 0.74 Selenium (mg/L) 0.0321 0.0326 1.55 Sodium (mg/L) 304 302 0.66 Sulfate (mg/L) 2290 2300 0.44 IDS (mg/L) 3920 3900 0.51 Uranium (mg/L) 0.0212 0.0212 0.00 Constituent MW-35 MW-70 %RPO 10/31/22 10/31/22 Bicarbonate as CaCO3 (mg/L) 305 272 11.44 Calcium (mg/L) 496 512 3.17 Chloride (mg/L) 60.6 67.2 10.33 Fluoride (mg/L) 0.305 0.245 21.82 Iron (mg/L) 0.21 0.23 9.09 Magnesium (mg/L) 158 163 3.12 Manganese (mg/L) 0.263 0.203 25.75 Potassium (mg/L) 10.8 11.1 2.74 Selenium (mg/L) 0.0121 0.0128 5.62 Sodium (mg/L) 361 371 2.73 Sulfate (mg/L) 2130 2190 2.78 IDS (mg/L) 3940 3830 2.83 Uranium (mg/L) 0.0223 0.0233 4.39 Radiologic Duplicate Tests Gross Alpha minus Rn & U* 3.26 3.71 0.63 Gross Alpha minus Rn & U Precision (±) 0.504 0.514 * Duplicate checks reported for gross alpha minus RN and U are not %RPD. Calculated values are based on the fonnula in the approved QAP. Per the approved QAP, an RPD greater than 20% is acceptable if the reported results are less than 5 times the RL. These results are provided for infonnation only. RPD exceeds the QAP limit of 20%. NIA -The duplicate test was not performed because both results were not greater than the RL. G 7B QA/QCE l -va uat10n or cce erate ti A amp,e up cates dS l D li MW-30 MW-65 Constituent 11/9/22 11/9/22 %RPD* Nitrate+ Nitrite (as N) (mg/L) 15.9 15.7 1.27 Selenium (mg/L) 0.0756 0.0768 1.57 Uranium (mg/L) 0.0101 0.0104 2.93 Chloride (mg/L) 156 183 15.93 MW-30 MW-65 Constituent 12/13/22 12/13/22 %RPD Nitrate+ Nitrite (as N) (mg/L) 16.1 15.2 5.75 Selenium (mg/L) 0.0708 0.0780 9.68 Uranium (mg/L) 0.0130 0.0126 3.12 Chloride (mg/L) 195 183 6.35 G-8A: Radiologies Counting Error Gross Alpha Counting Gross Alpha minus Rn and U Error::: Within Well Sample Date minus Rn & U Precision(+/-) 20¾ GWCL GWCL? MW-01 10/19/22 1.00 U 0.234 NC - MW-02 Resample 11101/22 1.03 0.292 N 3.2 y MW-03A 10/19/22 1.00 U 0.253 NC 7.5 NC MW-05 10112122 1.00 U 0.173 NC 3.75 NC MW-11 10/10122 1.00 U 0.225 NC 3.75 NC MW-12 10/13122 1.00 U 0.183 NC 7.5 NC MW-14 10/11/22 1.00 U 0.174 NC 7.5 NC MW-15 10/12122 1.00 U 0.319 NC 7.5 NC MW-17 10117122 1.00 U 0.236 NC 2.8 NC MW-18 10/18122 1.00 U 0.203 NC - MW-19 10/17122 1.00 U 0.272 NC - MW-20 11101/22 1.00 U 0.197 NC - MW-22 10119122 2.39 0.448 y - MW-23 11/01/22 1.00 U 0.285 NC 2.86 NC MW-24 11/02122 2.70 0.457 y 7.5 NIA MW-24A 11/02122 3.36 0.458 y - MW-25 10/10122 1.00 U 0.189 NC 2.86 NC MW-26 10/13122 1.50 0.317 N 4.69 y MW-27 10/19122 1.00 U 0.265 NC 4.69 NC MW-28 10112122 1.00 U 0.273 NC 2.42 NC MW-29 I 0112122 1.00 U 0.260 NC 2.42 NC MW-30 10113/22 1.00 U 0.302 NC 3.75 NC MW-31 10111/22 1.11 0.315 N 7.5 y MW-32 Resample 10131/22 1.85 0.421 N 3.33 y MW-35 10131/22 3.26 0.504 y 7.5 NIA MW-36 10/11122 1.00 0.293 N 7.5 y MW-37 11/01/22 1.00 U 0.283 NC 4.2 NC MW-38 11/01/22 1.00 U 0.206 NC - MW-39 Resample 11101/22 2.68 0.454 y - MW-40 10118122 1.04 0.290 N - TW4-24 11/01122 1.00 U 0.182 NC - MW-65 10/13/22 1.00 U 0.293 NC 7.5 NC MW-70 10131122 3.71 0.514 y 7.5 NIA NIA= the counting error is less than 20% of the activity as required by the GWDP and/or the value is above the GWCL and this check column is not applicable. NC= Not calculated. The sample results are nondetect and the check is not applicable. G-8B: Radiologies Counting Error for Accelerated Samples There are no accelerated samples collected for Gross Alpha. G-9A: Quarterly Sample Laboratory Matrix QC Matrix Spike % Recovery Comparison Lab Report Well Analyte MS%REC MSD%REC REC Range 22Jl 153 MW-25 Fluoride 75.3 75.2 80-120 22Jl 153 MW-11 Chloride* NC NC 80-120 22Jl 153 MW-11 Fluoride 75.0 76.2 80-120 22Jl 153 NA Chloride* NC NC 80-120 22Jl 153 NA Fluoride 136 128 80-120 22Jl 153 NA Chloride 58.3 59.0 80-120 22Jl 153 NA Chloride* NC NC 80-120 22Jl 153 NA Sulfate* NC NC 80-120 22Jl 153 MW-11 Sulfate 71.5 62.3 80-120 22Jl 153 MW-11 Nitrate 106 124 80-120 22J1703 MW-03A Calcium* NC NC 70-130 22J1703 MW-03A Sodium* NC NC 70-130 22J1703 MW-03A Magnesium* NC NC 70-130 22J1703 NA Calcium* NC NC 70-130 22J1703 NA Sodium* NC NC 70-130 22J1703 MW-03A Sulfate* NC NC 80-120 22J1703 NA Chloride* NC NC 80-120 22J1703 NA Sulfate* NC NC 80-120 22J1703 NA Chloride* NC NC 80-120 22J1703 MW-03A Sulfate* NC NC 80-120 22J1703 NA Chloride 56.3 57.7 80-120 22J1703 MW-03A Fluoride 71.3 78.1 80-120 22K0334 MW-35 Calcium* NC NC 70-130 22K0334 MW-35 Sodium* NC NC 70-130 22K0334 MW-35 Chloride 76.3 75.4 80-120 22K0334 NA Sulfate 106 153 70-130 22K0334 MW-35 Nitrate 141 134 80-120 22K0334 MW-35 Chloromethane 130 138 70-130 * Recovery was not calculated as the analyte level in the sample was greater than 4 times the spike amount. NA -QC was not performed on an EFRI sample. Method Blank Detections All Method Blanks for the quarter were non-detect. Laboratory Control Sample All Laboratory Control Samples were within acceptance limits for the quarter. Laboratory Duplicate % Recovery Comparison All Laboratory Duplicate samples were within acceptance limits for the quarter. Surrogate % Recovery All Surrogate recoveries were within acceptance limits for the quarter. RPD RPD Range 0.172 20 NC 20 NC 20 NC 20 3.80 20 0.138 20 NC 20 NC 20 2.76 20 4.39 20 NC 20 NC 20 NC 20 NC 20 NC 20 NC 20 NC 20 NC 20 NC 20 NC 20 0.467 20 8.16 20 NC 20 NC 20 1.05 20 9.76 20 5.11 20 5.74 20 --.. __ ------- G-98: Accelerated Laboratory Matrix QC M Spike% R C RPD Range Lab Report Well Aoalyte MS%REC MSD%REC REC Range RPD% % 22K0963 -November Monthly NA Chloride* NC NC 80-120 NC 20 22K0963 -November Monthly MW-I I Chloride* NC NC 80-120 NC 20 22K0963 -November Monthly MW-26 Chloride* NC NC 80-120 NC 20 22K0963 -November Monthly MW-26 Chloroform* NC NC 70-130 NC 20 22L 1318 -December Monthly MW-II Manganese* NC ** 70-130 ** ** 22L 1318 -December Monthly MW-II Sulfate* NC NC 80-120 NC 20 MW-65 (duplicate of 22LI 318 -December Monthly MW-30) Nitrate 69.3 86.9 80-120 1.10 20 22L 1318 -December Monthly MW-26 Chloroform 224 166 70-130 29.700 20 * Recovery was not calculated as the analyte level in the sample was greater than 4 times the spike amount ** CTF routine QC does not include a MSD for metals analyzed by 200.8. Precision is determined by other QC samples as allowable by the analytical method. NA -QC was not performed on an EFRI sample. Laboratory Duplicate % Recovery Comparison All Laboratory Duplicates were within acceptance limits for the quarter. Laborator_r_ Control Sample Lab Report Anal_rte LCS%REC REC Ran!!:e 22L 1318 -December Month Ir Sulfate 89 90-110 Method Blank Detections All Method Blanks for the quarter were non-detect. Surrogate % Recovery All Surrogate recoveries were within acceptance limits for the quarter. TabH Kriged Current Quarterly Groundwater Contour Map @ TW4-43 3:;:E 5523 TWN-20 []5564 TW4-42 ¢ 5524 estimated dry area temporary perched monitoring well installed September, 2021 showing elevation in feet amsl temporary perched nitrate monitoring well installed April, 2021showing elevation in feet amsl temporary perched monitoring well installed April, 2019 showing elevation in feet amsl MW-38 perched monitoring well "\>-5463 installed February, 2018 showing elevation in feet amsl M;-;504 perched monitoring well showing elevation in feet amsl i TW4-12 . . · 0 5568 temporary perched monitoring well showing elevation in feet amsl TWN-7 h d . . . A.5569 temporary perc e nitrate monitoring V well showing elevation in feet amsl PIEZ-1 perched piezometer showing "' 5588 elevation in feet amsl RUIN SPRING 6 5380 seep or spring showing elevation in feet amsl DR-06 . ( 54"92 MW-3W 1 Cell 48 :/ 5465 ~ DR-10 DR-11 . . 5482 5486 rtJ \ \ \ \ \ \ \ \ ' \ ' ' ' .... ab.,_,goned abangoned TWN-11 TWN'q O abanlfcned I r,/3;~, -~ TWiloB I PIEZ-01 alwlniofl"ld 'svs MW-19"" ,, ---,wfl<OS -.,, ---- / C ab•~"l)"d .£\, TW!li-12 u, 'IW~1 ~ ~-~,w~~-----5530 -, =~-----1 . .;, ~ --5525 5520 ~ I •I , '! I . I PIEZ-05 __'";-. ,1i 5510 ~, <J, I I '" r, 5500 5490 5480 5470 ' ,. .SJ9. :o R~h ~P~IN 1 mile " . _ .. ,---... •~"' • • ~ f"I ,.._ t· ., -.::.,.,..·.,1:~---..-::-..•.·,-,; NOTES: MW-4, MW-26, TW4-1, TW4-2, TW4-4, TW4-11, TW4-19, TW4-21 , TW4-37, TW4-39, TW4-40 and TW4-41 a.re chloroform pumping wells; TW4-22, TW4-24, TW4-25 and TWN-2 are nitrate pumping wells; TW4-11 water level is below the base of the Burro Ca.nton Formation HYDRO GEO CHEM,INC. KRIGED 4th QUARTER, 2022 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H:/718000/feb23/WL/Uwl1222.srf H-1 Tab I Groundwater Time Concentration Plots sa-34slNTERA Time concentration plots for MW-01 Chloride in MW-01 Sample Date Fluoride in MW-01 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 5000 4500 4000 3500 ~ 3000 'iio E "; 2500 ~ ~ 2000 1500 1000 500 0 ,. al - ' !/alll!:;~INTERA Time concentration plots for MW-01 ----. Sulfate in MW-01 ...._ ... --- Sample Date Uranium in MW-01 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ---~'IU • -,. -""'IP -- Detected Values Non-Detected Values Time concentration plots for MW-02 Chloride in MW-02 Sample Date Fluoride in MW-02 0.8 0 -1-------.------.-----..-----~---~------~---------I ".',°> oef s-¼INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 Detected Values ■ Non-Detected Values 20 18 16 14 ::;-12 .:a -= E 10 :, ·c ra .. 8 ::::> 6 4 2 0 ".'.°' tf 0 s--¥;1NTERA Time concentration plots for MW-02 Sulfate in MW-02 Sample Date Uranium in MW-02 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 80 70 60 ::;-so ....... ... .5. cu 40 :E l5 :E u 30 20 10 0 r::,'? r::,'1 ~ ~,,,~ .... ~ 1.8 1.6 1.4 1.2 ::;-....... ... 1 .5. cu :E l5 0.8 ::, ;::;: 0.6 0.4 0.2 0 r::,'? ::\ ~ ~r::, .... ~ ~'Ii s--2¥nlNTERA Time concentration plots for MW-03A Chloride in MW-03A Sample Date Fluoride in MW-03A Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 4500 4000 3500 3000 -::;-...... _g 2500 QI .... ~ 2000 "5 "' 1500 1000 500 0 ,;:,'> ,,_<:J" f::' ...,-s ~,,, 40 35 30 -25 ... "ii. ..:!: E 20 ::, 'i: I! ::> 15 10 5 0 ,;:,'> &-f::' ~,,,-( ...,-s ~94slNTERA Time concentration plots for MW-03A Sulfate in MW-03A Sample Date Uranium in MW-03A Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values ::, .. .s cu ~ 0 ::c u ::, ....... 140 120 100 80 60 40 20 0 'be ~,.->: Time concentration plots for MW-05 Chloride in MW-OS 'b"' 'b°' :0 (f '<"' 0 Sample Date Fluoride in MW-OS ! 1 ,111-----------------e,,--ll-l--4iili.-..-----------A--I cu "C -~ 0.8 :I ii: ~34.INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values ::::;-...... 9000 8000 7000 6000 "" 5000 .§. ! J!! 4000 :i .,, 3000 2000 1000 0 160 140 120 -100 -' ...... ... -== E 80 :::, ·2 I'!! ::::, 60 40 20 0 -Cl -L -- .--2#slNTERA Time concentration plots for MW-05 -- Sulfate in MW-OS ~ ---.. Sample Date Uranium in MW-OS --_e - Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ----~---~-,. - l!T - ' ; A ....__ Detected Values ■ Non-Detected Values ---34.INTERA Time concentration plots for MW-11 Chloride in MW-11 Sample Date Fluoride in MW-11 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-11 Sulfate in MW-11 0 +---~------r-----.,-----"T""---..-------.----~--------l c;'b"- ~o; -----¥slNTERA Sample Date Uranium in MW-11 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 Detected Values • Non-Detected Values 160 140 120 ::; 100 ...... .., .§. cu 80 "'Cl -~ ::c u 60 40 20 0 ,.:.~"' ~,,, 0.4 0.35 0.3 ::; 0.25 "oo .§. cu 0.2 !! :s :::, ;:.: 0.15 0.1 0.05 !c"\ ,_,.,q ~~INTERA Time concentration plots for MW-12 !')'\, :0 '<°' Chloride in MW-12 !';<o ,,.ss> ~ .,_, ~o ~s:,'? ~ Sample Date Fluoride in MW-12 -~ J lil Jl e - I Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 -v~ ■ j .:?"' 0 \ t, ( N J ' ~ ~ Detected Values Non-Detected Values Time concentration plots for MW-12 Sulfate in MW-12 9000 8000 ◄ 7000 6000 -::;- ] 5000 J!! £ 4000 :::, "' 3000 "--~ ~-,., - 2000 c~ ~-"y-Gf./1·----..,...,. ---tr"'/V 1000 30 25 20 -::;--.. -== E 15 :::, ·c 111 ~ 10 ~~INTERA ~ Sample Date Uranium in MW-12 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ' ■ ~) -- Detected Values Non-Detected Values Time concentration plots for MW-14 Chloride in MW-14 20 ::, 'bii .s OJ 15 :2 0 :c u 10 5 0 i-----,,------,----.-------,-----,-----.-----,----.------1 ~'tJ°' ~o ~-INTERA Sample Date Fluoride in MW-14 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 Detected Values • Non-Detected Values ::;--;;. E Time concentration plots for MW-14 Sulfate in MW-14 3000 -r--------------------------------- 2500 +----------------------------------1 "; 1500 ··••----------------------------------' ... J!! :i II) ::;-....... OD .a E :::, ·2 ~ ::::, 1000 +---------------------------------1 500 +--------------------------------J Sample Date Uranium in MW-14 120 100 80 60 40 20 Sample Date Detected Values .--¥slNTERA White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Non-Detected Values --"INTERA Time concentration plots for MW-15 Chloride in MW-15 Sample Date Fluoride in MW-15 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ■ Detected Values Non-Detected Values 70 60 50 ::; tin 40 .,:; E ::, ·2 30 ~ :::, 20 10 ~~INTERA Time concentration plots for MW-15 Sulfate in MW-15 Sample Date Uranium in MW-15 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ■ Detected Values Non-Detected Values Time concentration plots for MW-17 Chloride in MW-17 60 50 40 :;-....... 0.0 .s QI 30 "Cl -~ ::c u 20 10 0 +-----,----,-----,-------,----.-----,--------~-------1 ,._?J"> -.!-0 ~8:!INTERA Sample Date Fluoride in MW-17 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 Detected Values ■ Non-Detected Values Time concentration plots for MW-17 Sulfate in MW-17 O+-------.-----.------.----~---~---------------' ~°'"' ~'/j so 45 40 35 ~ 30 00 ..=: E 25 :I ·2 l"!! 20 ::::, 15 10 5 0 ~°'"' ~'/j ~-¥.INTERA Sample Date Uranium in MW-17 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 Detected Values • Non-Detected Values Time concentration plots for MW-18 Chloride in MW-18 0 +-----,------.----,--------.-----.----,--------.---~---1 ~ ...... i:°'"' ~'I> 0.45 0.4 0.35 0.3 00 .§_ 0.25 QJ :g 0.2 0 ::, ii: 0.15 0.1 0.05 0 !'J ;,."" ~'I> i:,"> .,r.; ~ ri--~INTERA Sample Date Fluoride in MW-18 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 Detected Values • Non-Detected Values -::;-....... "" -= E :::, ·2 "' ::i Time concentration plots for MW-18 Sulfate in MW-18 0 +-----.-----r-----.-----.----~--~---~------.J 5-:°'"' ~? 60 50 40 30 20 10 Sample Date Uranium in MW-18 0 +-----.-----.----r------.---~---r------.----~-------1 5-:°'"' ~'Ii Sample Date ~-#slNTERA White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ■ Detected Values Non-Detected Values 100 90 80 70 :::;-60 ...... CIO .§. QI 50 :2 l5 :c 40 u 30 20 10 0 i:0;"' ~'I> ~¼INTERA Time concentration plots for MW-19 Chloride in MW-19 Sample Date Fluoride in MW-19 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values ::;-....... tlD -== E :, ·2 "' ... ::::> Time concentration plots for MW-19 Sulfate in MW-19 o+---~---~---~--~-----------------...J ~°'"' ~'I> 30 25 20 15 10 5 Sample Date Uranium in MW-19 0 +----,----......... ------~---......... ---------------.I l' ~'I> Sample Date Detected Values ~-¥.INTERA White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Non-Detected Values .5--~INTERA Time concentration plots for MW-20 Chloride in MW-20 Sample Date Fluoride in MW-20 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ■ Detected Values Non-Detected Values Time concentration plots for MW-20 Sulfate in MW-20 ::. 12500 +-----,JC.... __________________________ _J .! J!! 2000 J.,E:....-------------------------------1 :i Ill Sample Date Uranium in MW-20 35 ::, 25 +------------,.'-------1--------------------l } E 20 +----------1--------A-----------------l ::, ·c ~ ::::, 15 +-----------------.J!ll.----------------1 ~"INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 Detected Values ■ Non-Detected Values 30 25 20 ::; ...... '"' g a, 15 :E l:i ::I ;::;: 10 5 ~s::.INTERA Time concentration plots for MW-22 Chloride in MW-22 Sample Date Fluoride in MW-22 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 60 50 40 ::::. tiii .,; E 30 ::, ·2 ~ ::::, 20 .... 3:slNTERA Time concentration plots for MW-22 Sulfate in MW-22 Sample Date Uranium in MW-22 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-23 Chloride in MW-23 -::;- .. 20 +---------------------------------..! .§. a, "0 "§ 15 +--------H-------------------------..1 ::c u Sample Date Fluoride in MW-23 0.9 ......--------------------------------- 0.8 -l-ll'-----------------------------------1 0.7 ------------------------------------1 0.6 -111;-----------------------------------l -::;-.. .§_ 0.5 a, "0 "§ 0.4 .,._. _______________ __.... _______________ __j :I u:: 0+---~-----.-------~---~-------------__j =----~INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 Detected Values • Non-Detected Values ::;- ~ E Time concentration plots for MW-23 Sulfate in MW-23 3000 -,--------------------------------- "; 1500 -1-11-1--------------1,I------------------...J ... ,l!! :i Ill 1000 -1--...--------------------------------l 500 -1---------------------------------...J 0 +--------.------.----------r----....--------------...J 90 80 70 60 ::;-...... ~ so E :I ·2 40 ~ ::) 30 20 10 0 @ I\ ~ ~r:; ..,-s ~'Ii ~~INTERA »°' ~'I,"( Sample Date Uranium in MW-23 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 Detected Values • Non-Detected Values 1.8 1.6 1.4 1.2 -::.-"'oa 1 .§. cu :5! l5 0.8 :I u:: 0.6 0.4 0.2 0 !.)., ~ ~ ~ ...,.s ...,.s ra-2¥.INTERA Time concentration plots for MW-24 !.)°' ~,,,.,,. Chloride in MW-24 Sample Date Fluoride in MW-24 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ■ Detected Values Non-Detected Values 250 200 ::::, 150 j E ::, ·2 ~ 100 so i ,le,,.,. 0 5--29#slNTERA Time concentration plots for MW-24 A.. Sulfate in MW-24 Sample Date Uranium in MW-24 - Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 - • -- Detected Values Non-Detected Values ~-::;INTERA Time concentration plots for MW-24A Chloride in MW-24A Sample Date Fluoride in MW-24A Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values ~-INTERA Time concentration plots for MW-24A Sulfate in MW-24A Sample Date Uranium in MW-24A Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 40 35 30 ::, 25 ...... 00 g QI 20 :g 0 :i: u 15 10 5 0 !:)" !:)'I ~ ~,.~ .... ~ 0.6 0.5 0.4 ::. ...... 00 g QI 0.3 :E ~ :::, Li: 0.2 0.1 ra,,--1$.INTERA Time concentration plots for MW-25 Chloride in MW-25 Sample Date Fluoride in MW-25 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-25 Sulfate in MW-25 ::i" 1200 -1----------------------------------1 ".a E 'a; 1000 -1----------------------------------1 ... J!! ~ 800 +-------------------------------------1 Po-:5¥.INTERA Sample Date Uranium in MW-25 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ■ Detected Values Non-Detected Values I 100 90 80 70 ::.-60 ...... co .§. QI so :5! 6 ::c 40 u 30 20 10 0 j:)1, j:)t,. c.,'l-<:i. q,<; <;) ~¥slNTERA Time concentration plots for MW-26 ~ /.: ~? Chloride in MW-26 Sample Date Fluoride in MW-26 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 0 S)'l, S)~ c.,l'I e" <:l 140 120 100 ::r ...... 80 Ill) -== E :::, ·2 60 ~ ::::, 40 20 ~%1NTERA Time concentration plots for MW-26 !:,:,,'I ~,. Sulfate in MW-26 ,;;°' 9/,...,..,, ~:-,°' :-,fo ~,."< '<~ 'l-~ ~o Sample Date Uranium in MW-26 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ~:-,'b 'l-Q. • :;:'1,<;; ?f,,,,,, ..,~ 0 Detected Values Non-Detected Values 60 so 40 ::, ....... "" .§. cu 30 :g 0 :E u 20 1 0.9 0.8 0.7 < 0.6 "" .§. cu o.s '0 ·;: 0 :::, 0.4 ii: 0.3 0,2 0.1 0 I:)., ~ ~ ~,.~ ...,-:s --S;INTERA Time concentration plots for MW-27 Chloride in MW-27 Sample Date Fluoride in MW-27 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values ~EG£;1NTERA Time concentration plots for MW-27 Sulfate in MW-27 Sample Date Uranium in MW-27 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 180 160 140 120 ::, ...... j 100 Ql :!2 l5 80 :i: u 60 40 20 0 <::,"> ~ ~ ~<::, ...,-s ~? 0.8 0.7 0.6 -0.5 -' ...... t>O .§. Ql 0.4 -0 ·;:: 0 :::, ii: 0.3 0,2 0.1 0 <::,"> <::,'\ ~ ~~ ...,-s .-34.INTERA Time concentration plots for MW-28 Chloride in MW-28 Sample Date Fluoride in MW-28 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 0 ~ ~ ~ ~'b~ ..,-s ~~INTERA Time concentration plots for MW-28 ~ ..,_q Sulfate in MW-28 Sample Date Uranium in MW-28 'S' ~ y ~❖ ~'Ii :0 ,,_e; :0 ,,_e; ~ ..,,,, Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ~ <J Qe; ■ ,¥~ '.\,'\, e:: ~o 0 Detected Values Non-Detected Values 45 40 35 30 ::.--r 25 QJ :5! l5 20 ::c u 15 10 5 0 ()" ()'\ ~ ~,,,---...,-s 0.8 ::.--11D .§. QJ 0.6 :g 0 :::, ;:;: 0.4 0.2 p,,--5=INTERA Time concentration plots for MW-29 Chloride in MW-29 Sample Date Fluoride in MW-29 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values Time concentration plots for MW-29 Sulfate in MW-29 -::;-'iii; 2000 +-------------------~-----------------..! .§. .l!! ~ 1500 +----------------llf-------------------1 :::, "' 60 so I 40 -::;- ---tlO -= E 30 :::, ·2 f! ::::, 20 -ft -- 10 r 4 0 ~¥zlNTERA Sample Date Uranium in MW-29 ...... ----- Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ----.., - • --V,V"V' r\. {!}'\, 0 Detected Values Non-Detected Values 0.5 ::. 'iii; 0.4 .§. 41 :5! l5 0.3 :::, u:: 0,2 0.1 0 !:)<, (\ If ,:'(<::, ...,-s ~'I> ~2¥.INTERA Time concentration plots for MW-30 Chloride in MW-30 Sample Date Fluoride in MW-30 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 1200 1000 800 ~ -bO .§. 600 cu .. .l!! :i Ill 400 200 ~-INTERA Time concentration plots for MW-30 Sulfate in MW-30 Sample Date Uranium in MW-30 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 450 400 350 300 ::.-...... I 2sa QI :2 l5 200 :i: u 150 100 so 0 ~" ~ ._,.;:; ::.-...... I a.s QI :2 Time concentration plots for MW-31 Chloride in MW-31 Sample Date Fluoride in MW-31 g 0.6 +--------1-ll----------~~--------.U...=-....!!!----1 ;:;: ~2¥slNTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 Detected Values • Non-Detected Values 1600 1400 1200 1000 -:;--1111 !. 800 a, ... ,l!! :i Ill 600 400 200 0 ~., 15' ~ ~ ....,-s ....,-s 30 25 20 -:;--"" -= E 15 ::, ·;: ns :) 10 Po::~INTERA Time concentration plots for MW-31 "',:,OJ ~'Ii Sulfate in MW-31 Sample Date Uranium in MW-31 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ■ Detected Values Non-Detected Values ----=c5 1NTERA Time concentration plots for MW-32 Chloride in MW-32 Sample Date Fluoride in MW-32 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ■ Detected Values Non-Detected Values Time concentration plots for MW-32 Sulfate in MW-32 Sample Date Uranium in MW-32 -::;-i4 ~-~~~----------------------------J E :::, -~ 3 f---1Hr➔-~l------------------------------l ::i ~2¥zlNTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 Detected Values • Non-Detected Values Time concentration plots for MW-35 Chloride in MW-35 80 70 60 -::;-50 'ii. .s GI 40 "Cl -~ :i: u 30 20 10 0 §> ~◊ <.: ~o; ~'I> Sample Date Fluoride in MW-35 -::;- 'ii. 0.4 'l------..-----t----------------lL.l,-----1"!1----6------1 .s GI :!:! g 0.3 +--------------l~-I--J---="=-+-=--1---,/---...\----I--+~.......:~~ il: s---sn5 INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 Detected Values ■ Non-Detected Values 35 30 25 ::. } 20 E ::, "i: 15 ~ ::::, 10 5 ,-5zlNTERA Time concentration plots for MW-35 Sulfate in MW-35 Sample Date Uranium in MW-35 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 0.6 0.5 0.4 ::;-....... "" ..§. cu 0.3 :!:! 5 :::, li: 0.2 0.1 ~¥.INTERA Time concentration plots for MW-36 Chloride in MW-36 Sample Date Fluoride in MW-36 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ■ Detected Values Non-Detected Values 30 25 20 ::; ....... tlO -== E 15 :I ·2 '" .. ::::, 10 5 r;.-34.INTERA Time concentration plots for MW-36 Sulfate in MW-36 ◊ tf 0 Sample Date Uranium in MW-36 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ■ Detected Values Non-Detected Values 60 50 40 -::;-...... .. .s CII 30 :!:! :s :i: u 20 ~2%slNTERA Time concentration plots for MW-37 Chloride in MW-37 Sample Date Fluoride in MW-37 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ■ Detected Values Non-Detected Values 20 18 16 14 ~ 12 .,. 2: E 10 :::, ·2 ~ 8 ::, 6 4 2 0 ❖ ~◊ ~ "?-.,j ~o p,,--$1NTERA Time concentration plots for MW-37 ~ :<i '<"' Sulfate in MW-37 Sample Date Uranium in MW-37 <, ,:I;...., ~,,, Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 50 45 40 35 < 30 ... ..s C11 25 3! l5 6 20 15 10 5 0 'b ~"' ,.. ... ,:,( ~'b ~o ~~INTERA Time concentration plots for MW-38 ,..~°' ~'b Chloride in MW-38 Sample Date Fluoride in MW-38 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values s--"INTERA Time concentration plots for MW-38 Sulfate in MW-38 Sample Date Uranium in MW-38 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 45 40 35 30 :.-...... .§'. 25 QI -0 "§ 20 ::c u 15 10 5 0 'b 'b ,i:_'> r::'> ~'I> 0 ~-¥.INTERA Time concentration plots for MW-39 {l ~ '?-q Chloride in MW-39 Sample Date Fluoride in MW-39 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 :-... r::"' 0 • r\. r::"' 0 Detected Values Non-Detected Values 16 • 14 12 -10 .... ....... "° -= E 8 ::I ·2 I'!! ::::, 6 4 2 0 'b 'b ,K"..; (f"..; ~'I, 0 s-S4slNTERA Time concentration plots for MW-39 Sulfate in MW-39 Sample Date Uranium in MW-39 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 0.9 0.8 0,7 0.6 ::;-....... "" .§. 0.5 cu :5! l5 0.4 :I u:: 0.3 0.2 0.1 0 'o 'o ,x-.; &-.; ~'I> 0 ~¥slNTERA Time concentration plots for MW-40 Chloride in MW-40 Sample Date Fluoride in MW-40 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 .... &"-' 0 • Detected Values Non-Detected Values 30 25 20 ::; ...... 00 ~ E 15 ::s ·2 .,, ::i 10 5 ra-¼INTERA Time concentration plots for MW-40 Sulfate in MW-40 Sample Date Uranium in MW-40 Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 • Detected Values Non-Detected Values 1400 1200 1000 ::.-...... 800 QO .§. QI 3! l5 600 ::c u 400 200 0 ,S, ~~°' ~ ...,-s ~'I> 0.6 0.5 0.4 ::.-...... QO .§. QI 0.3 3! l5 :::, ;::;: 0.2 0.1 0 'b ~:,,'b ~ .... ~'I> ~o Dl'-s.lNTERA Time concentration plots for TW4-24 ~..,,<::> ~o ~~ ~'I> Chloride in TW4-24 Y' l> ~<o '\ ~ ~"> ~ c}!..,, '?--s ~'I> ...,,,, 0 Sample Date Fluoride in TW4-24 ~ <::, ,,: ~o ~", ~'I> ~~ ~o ~,.,.,..,, ~'I> Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 ~ ~ ...,-s ~';I,..,, ~o • ~,.,.,..,, ~'I> ~,.,.,,.,., ~o ~,.,.,,.,., ~'I> ~,.,.,,.,., ~o Detected Values Non-Detected Values Time concentration plots for TW4-24 Sulfate in TW4-24 ~ 2500 1 ---~~----:,--------'=;:;;;;;;;;;;"d~:.__ ________ -j 'iii; E "'; 2000 +-_____ __,,.____ _______________________ ____J .... .l!! :; Ill 1500 +---------------------------------l Sample Date Uranium in TW4-24 800 ~ ...... l E 600 :I ·2 I!! ::::, 400 0 +------r---"'T"----~--~---~--~-----------J ,i:..,,<o ~,,, sa-"1!INTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring 4th Quarter 2022 Detected Values ■ Non-Detected Values TabJ CSV Transmittal Letter Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Goble, Kathy Weinel Tuesday, February 7, 2023 2:50 PM Phillip Goble 'Dean Henderson'; David Frydenlund; Scott Bakken; Garrin Palmer; Logan Shumway; Jordan Christine App Transmittal of CSV Files White Mesa Mill 2022 04 Groundwater Monitoring 04 2022 Analytical Data.csv; 04 2022 DTW all programs.csv; 04 2022 Field Data.csv Attached to this e-mail is an electronic copy of laboratory results for groundwater monitoring conducted at the White Mesa Mill during the fourth quarter of 2022, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel eF •:tt 'Mt• Energy Fuels Resources (USA) Inc. Kathy Weinel Director, Regulatory Compliance t:303.389.4134 I c: I t:303.389.4125 KWeinel@energyfuels.com 225 Union Blvd., Suite 600 Lakewood, CO 80228 http://www.energyfuels.com This e-mail ls Intended for the exclusive use of person{s) mentioned as the recipient(s). This message and any attached files with it are confidential and may contain privileged or proprietary information. If you are not the intended recipient(s) please delete this message and notify the sender. You may not use, distribute print or copy this message if you are not the intended reclpient(s). 1