The URL can be used to link to this page

Home My WebLink AboutDRC-2013-005142 - 0901a068804ae212Laboratories IIC a member of The GEL Group INC PO Box 30/12 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www gel com November 11, 2013 DRC-2013-005142 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: Tailings Soil Characterization Work Order. 336330 Dear Ms Weinel- GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on October 25, 2013 This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4505 Sincerely, fY; -rTli > -7 , t.Jh. ' Heather Shaffer Project Manager Purchase Order DW16138 Enclosures Energy Fuels Resources (USA), Inc. Tailings Soil Characterization SDG: 336330 Page 2 of 82 White Mesa Tailing Sample Results Boring Location Depth (ft) U-238 (pCi/g) Ra-226 (pCi/g) Th-230 (pCi/g) Pb-210 (pCi/g) 3-4N 6.5-7 24.7 149 62.2 91.1 8-9 29.4 153 58.4 120 10.5-11 25.7 230 120 105 2W4 5-6 22.9 385 200 362 8-9 47.4 749 708 485 11-12 146 678 525 555 13.5-14.5 23.7 735 493 653 16-17 46.3 826 514 960 2W3 6-7 62 946 554 858 7.5-8.5 98.7 482 448 980 9.5-10.5 35.8 635 428 884 13-14 9.79 166 176 133 2E1 5.5-6.5 6.39 294 124 2.34 12-13 14 656 295 458 17-18 13.8 531 199 320 23-24 16.6 146 122 100 26-27 15.3 328 142 249 3-6N 5-6 21.7 178 117 139 9-9.5 148 243 2240 238 13-14 262 1670 1390 1390 13-14D 251 1310 930 1360 16-17.5 185 1480 859 1230 2W2 7-8 75.1 913 728 1050 11.5-13.5 15.3 107 290 200 11.5-13.5D 44.2 553 427 740 16.5-17.5 41.9 648 349 675 2W6S(2) 11.5-12 24.9 1240 607 1040 12.5-13 56.2 276 219 204 14-14.5 123 1150 646 1360 2W6S(3) 14.5-15 54 623 706 900 16-17 50.8 505 473 576 Average Cone. 64.245 612.419 488.697 594.111 Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 336330 November 11, 2013 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843)556-8171 Summary: Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on October 25, 2013 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt Sample Identification: The laboratory received the following samples: Laboratory ID Client ID 336330001 3-4N6 5-7 336330002 3-4N 8-9 336330003 3-4N 10.5-11 336330004 2W4 5-6 336330005 2W4 8-9 336330006 2W4 11-12 336330007 2W4 16-17 336330008 2W4 13 5-14 5 336330009 2W3 6-7 336330010 2W3 7 5-8 5 336330011 2W3 9.5-10 5 336330012 2W3 13-14 336330013 2E1-5 5-6 5 336330014 2E1-12-13 336330015 2E1-17-18 336330016 2E1-23-24 336330017 2E1-6-27 336330018 3-6N 5-6 336330019 3-6N 9-9.5 336330020 3-6N 13-14 336330021 3-6N 13-14D 336330022 3-6N 16-17 5 336330023 2W2 7-8 336330024 2W2 11 5-13 5 336330025 2W2 115-13.5D 336330026 2W2 16.5-17.5 336330027 2W6-S(2) 11.5-12 336330028 2W6-S(2) 12 5-13 336330029 2W6-S(3) 14.5-15 Page 3 of 82 336330030 336330031 336330032 336330033 336330034 2W6-S(3) 16-17 2W6-S(2) 14-14.5 RIN 2W3 RIN 3-4N RIN 2W6-5(2) Case Narrative: Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package The enclosed data package contains the following sections Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions. Radiochemistry. f,. .'tjly ' -V., f.//< ' Heather Shaffer Project Manager Page 4 of 82 Project a GEL Quote i COC Number' PO Number Client Name r- s- , , i 4^-GEL Chain of Custody and Analytical Request GEL W ork Order Number: GEL Las.'rato'ies LLC IWO Savog? Roac C :iark$:u-). SC 2*437 Pho-c IWi> <56-fcI Pax. :8iJ "'•ft-i'.TS Sample Analysis Requested '5 .'F-'.l in i'ie rum her of containers for each tes:,i Project Site Name ii UJL., t . ./Ati,v >A.u 1 3V ' Address C'^Z^ £ H~-y i el I jSl-.-A^j. -T <3-iS« Should this sample b« considered Collected bv Send Results To Sample ID ' -->r composites - indicate start and stop aan^umi' Ct. •Ume (.* .Lt: .'J (mm-dd->> 1 (Military; Ihhmmj ^ in-pie \1alr-k " J •J Mi r, H °i Preservative Tvpe (6) Comments Note extra sample is -eqursd for sample specific QC HA/ 7 i-TlO 5 5 5 TAT Requested Normal Rush St>ecif\ No Crete Deliverab.c 1 of A QC S'jmnan Lc^i _cvei 3 •' Level 4 Remarks: Are there any kno* n hazards applicable to these samples 0 If so. please list the hazards Sample Co'tec'ion Time Zone Eastern Pacific Cen-a. Other ountatr Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished B> tSigned) Date Time Receued b> ,s'grcd! Date GEL PM '.e'.hoti of Shipmc-Date Sh'?peo A:roi! Airbill t 1 1 Chain of Custody Number - Client Detenrincd 2 ) QC Cooes N = Normal Sample TB = _-tp Blunt FD = I ie'd Duplicate E8 = Lqu nmer Blank MS = MJTIX Sp ke Sample MSD - Mai'.v Spike Jjpi ivt S ,-np<e 3) Field Filtered For liqjtd maimer md ea'e v.ilh a - \ - lor >c> *hc sample was f'cld fillerej or • • lo' sample v.as no! ' clc filtered 4) Mlt'ix Codes DW=Drinkin8 \v a'e' GW-Groundwaic- SW-Surface V.a.er \v W=\Vas:e *a er \v = o,a;e- SO=So'l SD-Scdin-e-.l SL=S Jdge SS-SoliJ'Aa^le O-Oii F-F,jer P-A'.pe I "-Ur.ne. K=FCCA! N-\asa^ 5) Sample Analys.s Requested Analvi'cal method requested I e «MOB MIOB^^tOl) mid runber p' ion.a.ners provide J fo- each 1 t *2SPB-1 Wl'iBTJ'1'* -1' 6) Preservative Type HA - Hvd-rKThlnr c Acic M - Nunc xcid. SH - Sod.un-Hvdramae. SA = Su ."vr 0 Mrid AA = Awo-pii ^.ij H\ * Hcxar'e ST - ^ojiur. 1 r.iosjl-a:; If -0 presc-vatnc IS ictxd - lea.c tielj b arl. r o> Lttb Receivtrg Lse Oriy Cut,ioa\ Seal i^iui-i0 YES MO Couter Temp C Page 5 of 82 WH1TF = I ARORATORY YELLOW = FILE PINK = CLIENT Page Project " GEL Quote « COC Number' PO Number GEL Chain of Custody and Analytical Request GEL Work Order Number- 3 ^ 3^) £) GLL L.at?ordto:;-cs, LLC 1,40 Sa\ a^c '-voac Cr>3r>cs'c-. aL ZWj- »k--c .'->-;'•' ?56-M~ 1 a. "rvr*. _ ' ~V Client Name ,—" „ , ._ .. ,. r i . Ph.ore : S c 74' Sample Analysts Requested tv :'ie ;11..T;r of cornamers for each test) Project-Site Name r\-v- I. ~V / V <. /Utj^ /A-il 4 >> <r "7>-:z-\ Address-/iZn, S Hi Should this sample be considtred Collected by £ j ^y .t-v^ t Send Resjits Tc Sample ID • For composites - .ndicatt* start ana stop uutc ti-n-i- -J- - L-l t.i.-J tmm-tld-w) tMilitlrv) ihnmml Sa-iip t Mir \ V) bJ <-- Hrei,tf-\-d!i vt Tv pe (61 *•» M -4 X) U a. Comments Note extra sample is required for sample specific QC o1 to i i ' ^ i VlC tC iz'lt3 2ivH Ifc-i7" TAT Requested Normal Rush Specify fax Results No Circle DelivcraDle C of A QC Su-nmar. LJ-CI 1 - L-vel2 • Leve: 3 Level- Remarks: Are there any known hazards applicable to these sarrpies0 If so. please list the hazards Sample Collection Time Zone Eastern Pacific Ceitrai Otber_ Chain of Custody Signatures Relinquished By {Signed) Dale Tine Sample Shipping and Delivery Details GEL PM Method of Shipncrt Date S^ippec Airbill = I ) Chain of Cus'ody Number - Clieni Determined I ) QC Codes N = Noma) Simple TB = Trip Blank FD = F-elJ Duplicate EB * L'quipner.' iilark MS * v|j-ri Spue Sample MSD » Matrix Sf'ke Duplica'e va-rp t O - (jra'p. C - Compos;'.- 3 ) Field Filtered For uquid matrices indicate vvilh a - \ - :or yes ihe sairple vvas '"tcld filivrej or - > • ti" sati'Pir was nei f.eld '-''*cred «) Mamx Codes DW-Drinking Mkatcr CW=Groundwa.er SW=Sur:ace VWer, WvV^VVas.e Wale' W-Aaie- SOSo'l SD-Scoimeni SL-S udsie SS'Sdid Aasle O"0il F-Fi'.er P=V.,pr hUn F»F.-;a N---Nasal 5) Sample Analysis Requested Analytical rrelnod requesied i-e 8260B. 60IOcv^470A) anj rLirtw- c' conra-ners provided tor cacF M : rlbOB-3 6"'rti ".'7'-t 1> 6 ) Preservative Type HA • -iydrocMinc Acid Nl = Nilr,. Acto. SH = Sod'um Hyd-ovioe SA " Su/ur.c Ac J ^A « Asc.vb-c AuJ H\ = Hi van; SI - S^J.J.n Thif salfaiv I; ou preservative is acoej = lea.; aelc hianx For Lcth Recerjmg Use Only Custody Seal In'.acP YES -\0 Cooler Temp C Page 6 of 82 WHITE = LABORATORY YELLOW = FILE PINK = CLIENT r"age. _ Project £ GEL Quote * COC Number' PO Number 1 of r-v.i GEL Chain of Custody and Analytical Request GEL Work Order Number: ^3 <g 3 ^ ^ Client Name £Atr^ t^cb Phone ~ ProjectvSite Name' Address Collected bv Send Results To |6 — H~y tO<s-*.~«-l Sample ID • For composites - indicate <lar: and s'op date lime •:>j.e C •! c te (mm-dd-vy) t '-.'kMrd iMtlitirvj thhmm) >an p'c Mir \ ,J GLL „aDci3W;>« [ LC HMO Sa-.j^-j •iinti Cia-lsston. SC 2v4C 7 Pho-ic i 'vi • i 55t>-J>. 7; fax : / 'mi- \ , Sample Analysis Requested 1 I i" inc lumber or comakers for each testj Should this sample he considered -A •it t-J c-4 X Preservative Type i,6) Comments Note: extra sample is required for sample specific QC Z v~- > y As L\.SI-OS±<ZA Q3 7-*'-s.s' icHv v W V^c,i lv.y v-iziji-S it. .s~a » v/ \ LM - ' I I -3 TAT Requested Normal Rush Specify iSubuc to sa-:ha-tei i ax Results Circle Deliverable C o: A QC Si.mr.ian. Level 2 . „evel 3 •' Level 4 Remarks: Are there any known hazards applicable to these samples0 If so, please list the hazards Sample Collection Time Zone L?stern Pacific Ccr.trai Other riKcuitam; Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished Bv (Signed) Daw Time Recptyd b. ii'gned> Da'e T.r = GEL PM Method of Sr-icrr.ent Date Sh'ppcG -\iritll i 1 ) Chain of Cuslodv Numbe- = Client Determ.ned 2 t QC Codes N = Normal Sample TB = T' p Blan« FD = ; led Dupl.calc EB = Leu pircnl ctlun* MS - M-V x Sp ki aamp.c M5D - Vnt'm sp-ne lXp.icjie Sarnie G •• tjrat C = C.'n poi.ic 3 ) held Filtered For liquid mat-ices indicate with a - v - -or yes tnc samp.e A as f,eid '~llcc* o' - - vr sa~ip e was rol fielj fliced 4) Matrix Codes DW»r>,nking Water CW<"-ound.iaier SW=Surfacc Water WW*»astc 'Aaicr w'Water SO=Soi SD'Sedimen . SL=Slvdge SS=S..liJ Vvas c 0=0 F^Fil'e- P=Wipc U-Lnnc. F-reci" N'Sasa 5 ) Sample Analysis Requested AnaUlical method requCSlec .1 t 8260B 6O10Br7470A I ar^j lu-rher p' cpnia'ners p-c.idcd Ux eacn .1 c - 3 6<nPB'~-t?04 • I i 6 1 PrtservanveTvpe HA - Hydrrchlonc Acid M - Nil-u Acid SH = Sodium hydrovidc SA - Sulfvic Acic AA = Asco-fcit. Ac.J H\ = •toaie ST = S^d.ur Th,osi, fait ll roorvserval ve .s added - leave 'elJ tvark Fvr Lob Receiving Lse Only I Custody Seal Intact7 ' iTS SO Cooler Temp I C Page 7 of 82 WHITE = LABORATORY YELLOW = FILE PINK = CLIENT Page j Project * V,\ GEL Quote = _ COC Number'1' PO Number Client Name of l GEL Chain of Custody and Analytical Request GEL \\ ork Order Number. Photic = OIL Labv rator e*. : 1C • 2i;4r. Sa.-iLti1 R.viJ C iai e<.s.- y"; ;»-»U7 Sample Analysts Requested "' i.Fili n .rr fttn'-e-nt'^rt-.aine'S fcr ea:n test) Project/ Site Name Tax = ^V- c t .<• lilt Address Should this s»mnle be considered. Collected bv Send Results To ^, U u',,,,< / Sample ID * For composites - indicate I'art ana slur dale l.'nc 'Date v - >!i*i (mm-dd-w i (Mii.tarvI >hhmml Preservative Type (6i Comments Note extra sample :s required for sample specific QC 2£ 1-5 5 - fc &' :|Z.j-3 i WvX 2£ i- t2-t i iesi. iu .-..guy : £ t -17 -1 *' \-\ZQ •;tt-2 2v l "1 x-> 7V v/ TAT Requested Normal Rush Specify tSuo e-l !•-> Su'chart:J i-aw Results No Circle Deliverable C of A QC Summary j.ci I Level 2 • Level : Level 4 Remarks: Are there any known hazards applicable to these samples'' If so. please ust the hazards Chain of Custody Signatures Sample Collection Time Zone Eastern Pacific Central Ol-er ATounlaujy} Sample Shipping and Delivery Details Relinquished B> (Signed) 1 iT^J^. C'.VU. Date Received bv isiynedi Dae 7'ine GEL ?M Method jf Shipment Date Snippec Airb'U« Al.'Dl'l 1 ) Cnain of Custody Number = Client Dc'cmmec 2 ) OC Codes N - Normal Sample TB - Trip B ar.k FH - r icld Duplicate EB " Ci;u.pmeii' BUnk MS = Vsl- \ Sp «e Sanp c MSD = .Mat'iv Sp i! Dvp.icaie SJ"ir.e C, - 'jra- C - fVmpos. e 3} FieldFiitered For liquid trainees, indicate wth a - V, . -or >cs the samp* vvas f.e.d liltced at - rv • >cnpie *as roi field :1 terse 4) Matrix Codes DW'Drmling Water GW-Gwid»aicr SW-Su-lace Waler WW=Waste M. ater W "V. a:er. SO=Soii SD-Sca.men SL=Slucge. SS^Soi d vS, as e O-Oi F-F. :e-. P=V. ipe L'-Line F=Fcc« S-Nasa1 5) Sample Analysis Requested Aralyucs mctr-od rcuues co u e 8260B 60IObV7470A ) ar.d -lumper o' contame-s provided 'or cac" M e -3 51 'W'l -It 6 ) Preservative Type HA - Hydrochloric Av.d M - Vrsc Acid SH = SodiLm Hvdrox.de SA - Sulfa".. 3cic AA - Asctvfc A:id H\ = Kcvan.- ST = Sod u n Thu'vu Luc . n,p-e«rva:->c s a-Jded - leave -'eld blanv For Lao Receiving Use Only Custody Seal Intact'' YES SO Cooler Temp C Page 8 of 82 WHITE = LABORATORY YELLOW = FILE PINK = CLIENT Page Project x GEL Quote * COC Number PO Number GEL Chain of Custody and Analytical Request GEL Work Order Number: v33^V^t3(7) GLL Labnra.o-es. ..L C 204:i Sava,;- Roa... hr-ieston. SC 2QJCT P-.cr,e fc'4ji 556-81 ~: rj\ ; *4 ? "\-ir\-I !"i Client Name »— _ . tr Ae y r-^vt-Vi Phone ' tlV ZZZX Project'Site Name Address ^' q S H S 11 Collected by t t- y „Vlt? -H Send Results To Sample ID ' For composites - indicate start and Stan dale lore "Da t J ' c ec tmm-dc-vA j I t 1: k'Ck'J (Mil.tan f ihhmmi r C,L San-pic Ma r y " Sample Analysis Requested ' n t.-.e number of containers for esch test; Should this sample be considered to •i tV ^— Preservative i ipc t6; Comments Note extra sample is required for sample specific QC i t Cr> .1-6 \,: iS-tH 11 ec iS'-iMfo' I J I ^Z-l I) I i \ ~2-C it- 17.SA I ilO TAT Requested Normal Rush Spec.fv Subiec >a-crjrt.-i Fay Results Yes Ctrc'e De.tverable C of A QC Summary Le. el Level 2 -' Level 3 1 Level 4 Remarks: Are there any known hazards applicable to these samples' If so. please list the hazards Sample Co'lection T.rne Zone Eastern Pacific Central Other -fT ^ ^v.cjr.'.Jm Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (S.gned) Date Time Received b\ > S'gr-ed 1 Dale TIT; GEL PM .Method of Shipment Dale Shipped A'tMii £ 1 ) Cham of Custody Number - Client Determined 2 ) QC Codes N = Norm*. Sample TB - Trip Blank FP ; I tM O ipbcaie F.B - I.cuirn.cni ULn* MS = VKir v Sn,*c- sunip.e MSD - Mu-."V Spike Duplicu'e S-mple C = .'jrafc C = Comsosne 3 } Field Filtered For iqvid matrices, indicate v*-lh a • V - -or ves lie ^an-pic v.as field Tilc-cd or - N - or sar"p.e v-tj r.oi ticld I.tiered 4) Matrix Codes DU-Drink'na, Waler C» =Groundvcaier SV. -Surface V. a er W vv = a, v. aier W-Wali' SO'Sm SD-Sed.ne-v SL'SI-dgc SS=So id 'A as c O-Oil F-riller P'Alpe l^U-inc F»lc-i>l rV=Aasa 5) Sample Analysis Requested Analytics' nicihod reuues'ed .e 8260B 60I0B/7470A 1 and nu<-Pcr o' ccntaine-s pro. dec! fo- each .t e i2t>r'd -3 *G 'nB<,~J''r>4 -li 6 ) Dreser>an\e Tjpe HA - Hydruth'onc Acid M = N, - c *cid SH - Sodn.m 'ysrov* S* ' Sulfu-u VciC A A = Asco-tic Acid H\ « hcxane ST - Sodiuir Th'osu'laic ro preset ai ce i added ' -ra-c '-e)d blank Far iab Receiving L'se Only Custody Seat Intact' YES NO Cooler Temp C Page 9 of 82 \\ H1TE = LABORATORY YELLOW = FILE PINK = CLIENT Page Project s GEL Quote « COC Number' PO Number L ... . .of. T>-...^ GEL Chain of Custody and Analytical Request GEL Work Order Number: 33^3v3t0 (GEL Laboratories, LLC 2040 Su<...ge ^ouJ 'CV.arie-i' SC 2->4-.T Uht-r.e (¥4." si6-» . 71 !fj\ 154.1, 1 r> Client Name — Phone = Sample Analysis Requested l_' .,F.I. ,n ire r jmber ol containers for each test; Project Site Name -~ uW^ >A.-ll fax^ Address T SH5II Should this Sam pit be considered Collected by ^t^y ,^\c - ^ Send Resul's lo Y-t\.\ t>-v i Sample ID ' '•'.v cofrpomcs - md'cait. s.jrt and ^ii>r '.vi:t' iimu {lnm-dd-v v: iMuitjr* I thhmmi sjrrn,. r-J ft j -- Preservative Tvpc • 6) Comments Note extra sampie is j requ red for sample specific QC : <~ 7-s" JjtlL \ u 1 E&l^ O 5 i <; — it.. > - i7.-S ; I Z ^ I > 3 ! i TAT Requested. Normal Rush Specif* ' SUJ CL li VJ'.1 J ^. ~a\ Results "ICS Cucie Deli.erasle C ot A QC ..-.el 2 Level 3 1 cvel 4 Remarks: Are there any known hazards applicable to these samples'' It so, please list the hazards Sarrr-e Co'iec: on T'tr-e Zone -.is.ern Pacific Cer:_irai O.he- C Sk'tii'tain. Chain of Custody Signatures Sample Shipping and Delivery Details Rehnqushed Bv iSigr.ecl Date Time Re.Aed b' ,v £r,c;. !GEL PM DQCC^es N = \rrrral Sarrrie TB ~ Trip T ark Ff> i id iJu-f <.3,-J FB "» j He d Fu'crec her i-qu d n:jiri^ss. indicate wih J - ^ - 'or ><:\ *i"c sjrrrlt. * i 4) Ma:r \ CixJci DW =L)I-m^ng * aic- GW-G rounds a cr SW-^r Aif- 5 J S3-np:: Vu-vys Rv-qjcsicti A^a -rc.il nen.-^ rc-^cilLd J SI&OB f>OEUB'~4',0A > j-tJ i 6 ' Prcser.3li.c T\pe H A " H". JncSljr'c *\<-.J M ^ V:r,; Aoc SH - Srd jm t WHITE - LABORATORY - ( Ni. -nitrn •t'.r^ Ms - \ . Clj tl. v.-2 I IT - N - • (*l v". f - /tL'.*? RcceivKg L <;e Only Cu\'.trJ\ Seal iiiaci7 .M.vl = ?..e '"ek. C Page 10 of 82 YELLOW = FILE PINK = CLIENT Page Project f GEL Quote => COC Number' PO Number of GEL Chain of Custody and Analytical Request GEL Work Order Number: s^v_3^?^*3^ GCL Laborutor.cs, LLC 2G40 Savage Read Charleston. SC 2y-'.'- Drvnv («•• *<6-S!7 IFxv <M3I "ff)-! '"8 Client Name Phone ~ M3S r 7jf ZZZi Project/Site Name T".v. I. ^ / L-OW.te .WtSc AA. U Fax*' Address V t-l .S ! Collected bv Sena Results To Sample ID * For ^orr.pusites - indicate Man and Mop Ja'e l'r, "Date Cr.lsvtc, (mm-dd-yv i • I .n. Oi'k.kJ tMilitarv) ftihmml Sai-ple Mat-v ,; Sample Analysis Requested ' iFti! .n 'be nuit^e: of contai.te-s for each lest) Should this | i SJmple he ' 'x M rJ 2 N M -Jl rj hi •— Preservative T>ne (6) Comments Note, extra sample is required for sample specific QC v, A.ji.i,J;A i g tc is- 2. - S ("•?) t-.-v-K I 22.1.3 ! J -iiS 20fe-S.z) t-CM.S tci ZA j I ? l JJC TAT Requested- Normal- Rush Specify iSa'-ic-t • Sur:-iargn |Tax Results T es No ', Crclc Deliverable C of A ' QC Summary Level 1 . Level 2 • Level 3 Level 4 Remarks: Are there anv knos\ n hazards applicable to these samples'' U so please list the hazards jSample Collection Time Zone I Las.em Pacific I Get—a Other Chain of Custody Signatures Sample Shipping and DehveryDelails Relinquished By (Signed) Date Time Received bv isi^ed' Date Tine 'GEL PM Me'hod ot Sh'pneri Da*e Sr-.nned {Arh.il • I t Chain of Custocy Surubcr = Client Determined : IOC Codes N - Nonrul Sample TB ' T'lp Blank FD » Fie d Duplica'e EB = Equ.pme- B.ank MS = vtv.-v Sr.,e Simple MSD - vtair.v Spike J.'pKa.e Sarrp e C -- ti'ub. C = C ompos. ; 3 ) Field Filtered For liqaid matrices indicate with a - Y - lor ves he vlmple *as r,cld fi'icred or - N - 'o' sar-plr wav not t-e'd ''il'cre:! 4) Mal'ix Codes DW'Onri^rig V, o:c. CW=Groundv.ule- SW ^Surface VVa'e- WW'Waite Vva er W-Aaier SO-So.l SD-Sedin-tm SI.=S udgv SS-SoliC Waste 0=OH F=Fiiier r" = Vs pe I -Ur ne. F=rec,V N = Saaai 5) Sample Analysis Requested Anaiv real methoo requested h e 8260B MIOB/^TJA) a.id ru -ibe- cvn a ncrs proviccd .p- each l; e a.'ci1^ - 3 tf,;'>&r^<>* -Ji 6 J Presetvafve Type HA - Hvdrochlorc \cid Nt = Sun. Ac.d. SH * Soo um Hydrov.de SA = Su i\.-c A.'a A A - Asccrbi. And H\ = Hcvane ST = Soda m 1 mosuliul: il no p'ese'v ativt is aoced » 'eave iieL lv ar« vO' Ljh Receding Use Q"ly Custody Sea! intact7 YES SO Cooler Temp C 11 of 82 WHITE = LABORATORY YELLOW = FILE PINK = CLIENT Page Project GEL Quote s COC Number' PO Numbei of _i_ _:2-ij-f_ GEL Chain of Custody and Analytical Request GEL Work Order Number: <>l'.. I aftora'-.nev. LLC 204 } Sa.uiie Roae L ha-ies'nn, SC Zl'i^:.'~ l- Cltent Name Af- '> > b v •• 'J P'n.vie =• ,7i IUI Sample Analysis Requested '•' • b:i in the r^i-iber r>- U'r.ta'ners :~cr each tes:; ProjectSite Name •~< l-rV>> i i ! ^k. U .-w.-tl. Fax* Address Should this sample he considered Collected bv Send Results To Sample ID or composUes - ina\cctc Mart and •a-->pju\ ji^-j-Uy ~c 1 •Da.cC-lc.-ed 1 mm-dd-w. ( •>. echo iMllltarv r Ihhmm I 01 t .. e, I .... • .li..e-ei" -.anisic Malr.s <1 >r Preserva'....'e Type (6) Comments Note, extra sample is required for sample specific QC id 2-< 1 • j> it t"> As; ,i,i^aJt.l ^.Hy RrV VIA/ v/> C^ t.. ,£U5li3 li=>£ TAT Requested- Normal Rush Specify (Suhieci Surcharge! jbax Res-.:> res No Circle Deliverable Cot* A QC Stiinmarv Level 1 . Level 2 / Level 3 / Level 4 Remarks: Are there any known hazards applicable to these samples'' If so please list the hazards Sample Collection Time Zone ; Eastern Pacific j CentnL Other {. Mountain Chain of Custody Signatures Relinquished By (Signed) Date 1 6 ^IZ^'l Time Received b. (s'gnec Date 1-ne Sample Shipping and Delivery Details C.EL PM Method of Sh piner Date Sn-rned I Airbill - 1 ) Chain of Custody Nurrber = Client Determined 2 ) QC Codes S - Normal Sample TB - Ino BlBnk. FD • f ield Duplicate, FB - Lqu pmi 1 IVui-fc MS = Vlair * Sp-kc S..r ple. MSD = Mal-'v Spue J„pncat= suiTfe C ' Grab C - ( ompus'te 3 ) Field Filtered For liquid matr.ces ma.cale »tin a - V • lor ves the sample ^as feld fil-c-ei or - > - sui-oic *K not r,;«j 'i1 :ted 4) Matrix Cooes DW-Dnnkmg Watc GVV-Croundwa.cr SW=Surface Water. WW=Wastc Vvaier. W^Water SO-So'l SD-Scdimen SL-s udge. SS'Splic Aaste 0>0. F'Fi! rr P'Wipe l»Lrnt, F=re.v Nasal 5) Sample Analysis Requested Analytical pie'h.od reouesled n e J260B 6OI0B/7470A) ard r.u nbe-containers provided r,-i each n : WIS - 5 -I) 6 ) Preservative Tvpc HA - Hydrocnloric vcid M = Nit-i. \c.d SH = Sodium H\drc».d-. SA • bu! ur.v.'d A A - As.o-bic Acd HX - Hevne ST - S. d.un. 1 nicsulalc it no prescrva'ivc is added - 'ca-e tide blank r-ir Lac Receiving Use Only Custody Seal Intact7 YES -V0 Page 12 of 82 WHITE = LABORATORY YELLOW = FILE PINK = CLIENT GEL Laboratories LLC \VT SAMPLE RECEIPT & REVIEW FORM SPG/AR/COCAVork Order: 3\?)<C> 3 3D Received By: "^T^ KQ -*M\jT Date Received: (^ ^ . 2. S, I 2> If Net CounU > 1 OOcpm on samplesnot marked "radioactive", contact the Radiation Safety Croup for further investigation. Suspected Hazard Information 1 COC/Samples marked as radioactive? Maximum Net Counts Observed* (Observed Counts - Area Background Counts): j\\ Classified Radioaciive II or III by RSO? If yes, Were swipes taken of sample containers < action levels'7 COC/Samplcs marked containing PCBs? Package, COC, and/or Samples marked as beryllium or asbestos containing? If yes, samples are to be segregeated as Safety Controlled Samples, and opened by the GEL Safety Group. Shipped as a DOT Hazardous? Hazard Class Shipped: UN#: Samples identified as Foreign Soil? Sample Receipt Criteria Comments/Qualifiers (Required for Non-Conforming Items) Shipping containers received intact and sealed? Circle Applicable: Seals broken Damaged container Leaking container Other (describe) Samples requiring cold preservation within (0 < 6 deg. C)7* 1 Preservation Method Ice bags Blue ICC Dry ice None Olher (describe) •all temperatures are recorded in Celsius Za Daily check performed and passed on [R temperature gun? X Temperature Device Serial H Secondary Temperature Device Serial It (If Applicable). j ^ ^ Chain of custody documents included with shipment? Sample containers intact and scaled? Circle Applicable Seals broken Damaged container Leaking container Olhci (describe) Samples requiring chemical preservation at proper pH? Sample ID'S, containers affected and observed pH' If Preservation nrided. VOA vials free of hcadspacc (defined as < 6mm bubble)? Sample ID'S and containers affected' Arc Encore containers present? (If yes, immediately deliver to Volatile! laboratory) Samples received within holding time? ID'S and tests affected' Sample ID's on COC match ID's on bottles? Sample ID's and container! affected' 10 Date & time on COC match date & time on bottles? Sample ID'S affected' 11 Number of containers received match number indicated on COC? Sample ID's affected' 1^^ f^c'£ (J ) £oo\; C. In i^f X ?J NMAl' 3 S-1 0 HOT o fo CjhQ. p, >. 12 Are sample containers identifiable as GEL provided? 13 COC form is properly signed in relinquished/received sections? n 14 Carrier and tracking number. Circle Applicable: FedEx Air FedEx Ground UPS Field Services Courier Other I031 szfcp <33 Comments (Use Continuation Form if needed) PM (or PMA) review. Initials Date Page. ' of GEL Laboratories LLC - Login Review Report GEL Work Order/SDG: 336330 Client SDG: Project Manager: Project Name: Purchase Order: Package Level: EDD Format: 336330 Heather Shaffer DNMI00107 Tailings Soil Characterization DW16138 LEVEL3 EIM DNMI Work Order Due Date: 14-NOV-13 Package Due Date: 12-NOV-13 EDD Due Date: 14-NOV-13 Due Date: 14-NOV-13 HXS1 Report Date 11-NOV-13 Work Order 336330 Page 1 of 8 Collector: C Prelogin #: 20131009645 Project Workdef ID: 1330584 SDG Status: Closed Logged by: GEL ID Client Sample ID Client Sample Desc. Collect Date & Time Receive Time # of Date & Time Zone Cont. Lab Matrix Fax Days to Due Date Process CofC# Prelog Lab Field Group QC QC 336330001 336330002 336330003 336330004 336330005 336330006 336330007 336330008 336330009 336330010 336330011 336330012 336330013 336330014 336330015 336330016 336330017 336330018 336330019 336330020 336330021 336330022 336330023 336330024 336330025 336330026 336330027 336330028 336330029 3-4N 6 5-7 3-4N 8-9 3-4N 10 5-11 2W4 5-6 2W4 8-9 2W4 11-12 2W4 16-17 2W4 13 5-14 5 2W3 6-7 2W3 7 5-8 5 2W3 9 5-10 5 2W3 13-14 2E1-5 5-6 5 2E1-12-13 2E1-17-18 2E1-23-24 2E1-6-27 3-6N 5-6 3-6N 9-9 5 3-6N 13-14 3-6N13-14D 3-6N16-17 5 2W2 7-8 2W2 11 5-13 5 2W2 11 5-13 5D 2W2 16 5-17 5 2W6-S(2) 11 5-12 2W6-S(2) 12 5-13 2W6-S(3) 14 5-15 22-OCT- 22-OCT- 22-OCT- 21-OCT- 21-OCT- 21-OCT- 21-OCT- 21-OCT- 21-OCT- 21-OCT- 21-OCT- 21-OCT- 21-OCT- 21-OCT- 21-OCT- 21-OCT- 21- OCT- 22- OCT- 22-OCT- 22-OCT- 22-OCT- 22-OCT- 22-OCT- 22-OCT- 22-OCT- 22- OCT- 23- OCT- 23-OCT- 23-OCT- 13 13 10 13 1320 13 13 30 13 1525 13 15 30 13 1540 13 1600 13 1550 13 16 35 13 16 40 13 16 55 13 17 05 13 14 00 13 14 10 13 14 20 13 14 35 13 14 50 13 10 50 13 11 05 13 11 20 13 11 20 13 11 30 13 09 20 13 08 35 13 08 35 13 08 55 13 10 00 13 10 10 13 09 05 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 25-OCT- 13 0910 13 09 10 13 09 10 1309 10 1309 10 1309 10 13 09 10 -2 13 09 10 -2 13 09 10 -2 13 09 10 -2 13 09 10 -2 13 09 10 -2 1309 10 13 09 10 13 09 10 13 09 10 13 09 10 13 09 10 1309 10 1309 10 13 09 10 -2 13 09 10 -2 13 09 10 13 09 10 13 09 10 13 09 10 13 09 10 13 09 10 13 09 10 SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID SOLID 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 C4. 00 OJ 00 C3 a, GEL Laboratories LLC - Login Review Report 336330030 2W6-S(3) 16-17 336330031 2W6-S(2) 14-145 336330032 RIN 2W3 336330033 RIN 3-4N 336330034 RIN 2W6-5(2) 23-OCT-13 09 25 25-OCT-13 09 10 -2 23-OCT-13 10 30 25-OCT-13 0910 -2 21- OCT-13 15 15 25-OCT-13 09 10 -2 22- OCT-13 13 00 25-OCT-13 09 10 -2 23- OCT-13 10 50 25-OCT-13 09 10 -2 SOLID SOLID WATER WATER WATER 20 20 20 20 20 Report Date 11-NOV-13 Work Order 336330 Page 2 of 8 Client Sample ID Status Tests/Methods Product Reference Fax Date PM Comments Aux Data Receive Codes -001 3-4N6 5-7 -002 3-4N 8-9 -003 3-4N 10 5-11 -004 2W4 5-6 -005 2W4 8-9 -006 2W4 11-12 -007 2W4 16-17 -008 2W413 5-14 5 REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, PB210, Solid REVW Lucas Cell, DOE Ra-04. Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid Cooler Seal Undisturbed Y Temperature (C) 23 Cooler Seal Undisturbed Y Temperature (C) 23 Cooler Seal Undisturbed Y Temperature (C) 23 Cooler Seal Undisturbed Y Temperature (C) 23 Cooler Seal Undisturbed Y Temperature (C) 23 Cooler Seal Undisturbed Y Temperature (C) 23 Cooler Seal Undisturbed Y Temperature (C) 23 Cooler Seal Undisturbed Y RAD1 RAD1 RAD1 RAD1 RAD1 RAD1 RAD1 RAD1 CM CO 0, GEL Laboratories LLC - Login Review Report -009 2W3 6-7 -010 2W3 7.5-8.5 -011 2W3 9 5-10 5 -012 2W3 13-14 -013 2E1-5.5-6.5 -014 2E1-12-13 -015 2E1-17-18 -016 2E1-23-24 REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid Temperature (C) 23 Report Date 11-NOV-13 Work Order 336330 Page 3 of 8 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y RAD1 CO VO ID DO CO 0-, GEL Laboratories LLC - Login Review Report -018 3-6N 5-6 -019 3-6N 9-9 5 -020 3-6N13-14 -021 3-6N13-14D -022 3-6N 16-17.5 -023 2W2 7-8 -024 2W2 11 5-13.5 -025 2W2 11.5-13.5D -026 2W2 16.5-17.5 REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226. solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th. Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210. Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th. Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid Temperature (C) 23 Report Date-11-NOV-13 Work Order 336330 Page 4 of 8 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 Cooler Seal Undisturbed RAD1 CO o r~- <u c>0 03 GEL Laboratories LLC - Login Review Report -027 2W6-S(2) 11.5-12 -028 2W6-S(2) 12.5-13 -029 2W6-S(3) 14.5-15 -030 2W6-S(3) 16-17 -031 2W6-S(2) 14-14 5 -032 RIN2W3 -033 RIN 3-4N -034 RIN 2W6-5(2) REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Solid REVW Alphaspec U, Solid REVW GFPC, Pb210, Solid REVW Lucas Cell, DOE Ra-04, Ra226, solid REVW Alphaspec Th, Liquid REVW Alphaspec U, Liquid REVW GFPC, Pb210, Liquid REVW Lucas Cell, DOE Ra-04, Ra226, liquid REVW Alphaspec Th, Liquid REVW Alphaspec U, Liquid REVW GFPC, PD210, Liquid REVW Lucas Cell, DOE Ra-04, Ra226, liquid REVW Alphaspec Th, Liquid REVW Alphaspec U, Liquid REVW GFPC, Pb210, Liquid REVW Lucas Cell, DOE Ra-04, Ra226, liquid Report Date 11-NOV-13 Work Order 336330 Page 5 of 8 Temperature (C) 23 Cooler Seal Undisturbed Y Temperature (C) 23 Cooler Seal Undisturbed Y Temperature (C) 23 Cooler Seal Undisturbed Y Temperature (C) 23 Cooler Seal Undisturbed Y Temperature (C) 23 Cooler Seal Undisturbed Y Temperature (C) 23 RAD1 RAD1 RAD1 RAD1 RAD1 Cooler Seal Undisturbed Y Temperature (C) 23 Cooler Seal Undisturbed Y Temperature (C) 23 Cooler Seal Undisturbed Y Temperature (C) 23 GEL Laboratories LLC - Login Review Report Product: LUC26RA04S Workdef ID: 1330592 Method: DOE EML HASL-300 Ra-04 Product Description: Lucas Cell. DOE Ra-04, Ra226, solid In Product Group? No Group Name: Group Reference: Samples 001, 002, 003, 004, 005, 006, 007, 008, 009, 010, 011, 012. 013. 014, 015, 016, 017, 018, 019, 020, 021, 022, 023, 024, 025, 026, 027, 028, 029. 030, 031 Parmname Check: All parmnames scheduled properly Report Date 11-NOV-13 Work Order 336330 Page 6 of 8 Path: DOE Ra-04 Product Reference: Moisture Correction: "Dry Weight Corrected" CAS# Parmname Client RDL or Reporting Parm Included Included Custom PQL & Unit units Function in Sample? in QC? List? 13982-63-3 Radium-226 pCi/g REG No Product: ASP_THS Workdef ID: 1330586 In Product Group? No Method: DOE EML HASL-300, Th-01-RC Modified Product Description: Alphaspec Th, Solid Group Name: Group Reference: Samples: 001, 002, 003, 004, 005. 006, 007. 008, 009, 010, 011, 012, 013, 014, 015, 016, 017, 018, 019, 020, 021, 022, 023, 024, 025, 026, 027, 028, 029, 030, 031 Parmname Check: All parmnames scheduled properly Path: No Ash pCi/g Product Reference: Moisture Correction: "Dry Weight Corrected" CAS# Parmname Client RDL or PQL & Unit Reporting Units Parm Included Included Custom Function in Sample? in QC? List? 14269-63-7 Thorium-229 Tracer Thorium-230 pCi/g pCi/g SURR REG Yes Product: LUC26RA04L Workdef ID: 1330591 Method: DOE EML HASL-300 Ra-04 Product Description: Lucas Cell, DOE Ra-04, Ra226, liquid Samples: 032. 033, 034 Parmname Check: All parmnames scheduled properly CAS# Parmname In Product Group? No Group Name: Client RDL or PQL & Unit Reporting Units Group Reference: Path: Ra-04 Product Reference: Moisture Correction: "As Received" Parm Included Included Custom Function in Sample? in QC? List? 13982-63-3 Radium-226 pCi/L REG No Product: GFC PBL Workdef ID: 1330589 Method: DOE RP280 Modified Product Description: GFPC, Pb210, Liquid Samples: 032, 033, 034 Parmname Check: All parmnames scheduled properly CAS# Parmname In Product Group? No Group Name: Client RDL or PQL & Unit Reporting Units Group Reference: Path: Standard Product Reference: Moisture Correction: "As Received" Parm Included Included Custom Function in Sample? in QC? List? 14255-04-0 Lead-210 5 pCi/L REG Y Y No GEL Laboratories LLC - Login Review Report Report Date H-NOV-13 9 Work Order 336330 Page 7 of 8 Product: GFC PBS Workdef ID: 1330590 In Product Group? No Group Name: Group Reference: Method: DOE RP280 Modified Path: Standard Product Description: GFPC, Pb210, Solid Product Reference Samrjles 001 • 002' 003' °04' 005' 006' 007' °08' 009' 01°- 011 • °12- 013' 0U' 015' 016' 017' 018- 019' 020' 021 • °22- 023' °24- Moisture Correction' "Dry Weight Corrected" P ' 025,026,027,028,029.030,031 Parmname Check: All parmnames scheduled properly Client RDL or Reporting Parm Included Included Custom CAS # Parmname PQL & Unit Units Function in Sample? in QC? List? 14255-04-0 Lead-210 5 pCi/g REG Y Y No Product: ASP THL Method: Product Description: Samples Parmname Check: CAS# Workdef ID: 1330585 In Product Group? No DOE EML HASL-300, Th-01-RC Modified Alphaspec Th, Liquid 032, 033, 034 All parmnames scheduled properly Parmname Group Name: Client RDL or PQL & Unit Reporting Units Group Reference: Path: Standard Product Reference: Moisture Correction: "As Received" Parm Included Included Custom Function in Sample? in QC? List? 14269-63-7 Thonum-229 Tracer Thonum-230 pCi/L pCi/L SURR REG Y Y Yes Product: ASP_UUL Method: Product Description: Samples. Parmname Check: CAS# Workdef ID: 1330587 In Product Group? No DOE EML HASL-300, U-02-RC Modified Alphaspec U, Liquid 032, 033, 034 All parmnames scheduled properly Parmname Group Name: Client RDL or PQL & Unit Reporting Units Group Reference: Path: Standard Product Reference- Moisture Correction: "As Received" Parm Included Included Custom Function in Sample? in QC? List? 14158-29-3 7440-61-1 Uranium-232 Tracer Uranium-238 pCi/L pCi/L SURR REG Yes Product: ASP_UUS Method: Product Description: Samples' Parmname Check: CAS# Workdef ID: 1330588 In Product Group? No Group Name: Group Reference: DOE EML HASL-300, U-02-RC Modified Alphaspec U, Solid 001, 002, 003, 004, 005, 006, 007, 008, 009, 010, 011, 012, 013, 014, 015, 016, 017, 018, 019, 020, 021, 022, 023, 024, 025, 026, 027, 028, 029, 030, 031 All parmnames scheduled properly ' " Reporting Path: Standard Product Reference- Moisture Correction: "Dry Weight Corrected" Client RDL or Parmname PQL & Unit Units Parm Included Included Custom Function in Sample? in QC? List? 14158-29-3 7440-61-1 Uranium-232 Tracer Uranium-238 pCi/g pCi/g SURR REG Y Y Yes oo o fN o CJ) C3 CL, GEL Laboratories LLC - Login Review Report Report Date II-NOV-I3 a K Work Order 336330 Page 8 of 8 Action Product Name Description Samples Contingent Tests Login Requirements: Requirement Include7 Comments Peer Review by.. Work Order (SDG#), P0# Checked?. C of C signed in receiver location? List of current GEL Certifications as of 11 November 2013 State Certification Alaska UST-110 Arkansas 88-0651 CL1A 42D0904046 California NELAP 01151CA Colorado SC00012 Connecticut PH-0169 Delaware SC000122013-10 DoD ELAP/1 SO 17025 A2LA 2567 01 Florida NELAP E87156 Foreign Soils Permit P330-12-00283, P330-12-00284 Georgia SC00012 Georgia SDWA Hawaii 967 SC000122013-10 Idaho Chemistry SC0O0I2 Idaho Radiochemistry SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky 90129 Louisiana NELAP 03046(A133904) Louisiana SDWA LA 130005 Maryland 270 Massachusetts M-SC012 Michigan 9976 Mississippi SC000122013-10 Nebraska NE-OS-26-13 Nevada SC0001220I3-2 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 Oklahoma 9904 Pennsylvania NELAP 68-00485 Plant Material Permit PDEP-12-00260 South Carolina Chemistry 10120001 South Carolina GVL 23611001 South Carolina Radiochemi 10120002 Tennessee TN 02934 Texas NELAP T104704235-13-8 Utah NELAP SC000122013-I1 Vermont Virginia NELAP VT87156 460202 Washington C780-12 Wisconsin 999887790 Page 22 of 82 Radiochemistry Case Narrative Energy Fuels Resources (DNMI) SDG 336330 Method/Analysis Information Product: Alphaspec Th, Liquid Analytical Method' DOE EML HASL-300, Th-01-RC Modified Analytical Batch Number. 1341943 Sample ID 336330032 336330033 336330034 1202974872 1202974873 1202974874 Client ID RIN 2W3 RIN 3-4N RIN 2W6-S(2) Method Blank (MB) 336330032(RIN 2W3 ) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-038 REV# 16. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met Standards Information Standard solutions for these analysis are N1ST traceable or verified with a NIST traceable standard and used before the expiration dates Sample Geometry All counting sources were prepared in the same geometry as the calibration standards Quality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 336330032 (RIN 2W3 ). QC Information All of the QC samples met the required acceptance limits Page 23 of 82 Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time Sample Re-prcp/Rc-analysis None of the samples in this sample set required reprep or reanalysis. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Manual Integration Manual integrations of alpha spectroscopy spectra 1202974873 (RIN 2W3 ), 336330032 (RIN 2W3 ) and 336330033 (RIN 3-4N) were performed to fully separate counts in Regions of Interest which would have been biased Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required. Method/Analvsis Information Product: Alphaspec U, Liquid Analytical Method. DOE EML HASL-300, U-02-RC Modified Analytical Batch Number: 1341944 The samples in this SDG were analyzed on an "as received" basis SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP) The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-011 REV# 24 Sample ID 336330032 336330033 336330034 1202974875 1202974876 1202974877 Client ID RIN 2W3 RIN 3-4N RIN 2W6-S(2) Method Blank (MB) 336330032(RIN 2W3 ) Sample Duplicate (DUP) Laboratory Control Sample (LCS) Page 24 of 82 Calibration Information: Calibration Information All initial and continuing calibration requirements have been met Standards Information Standard solutions for these analysis are N1ST traceable or verified with a N1ST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control fOC) Information: Blank Information The blank volume is representative of the sample volumes in this batch. Designated QC The following sample was used for QC: 336330032 (RIN 2W3 ) QC Information All of the QC samples met the required acceptance limits Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time Sample Re-prep/Re-analysis Sample 1202974875 (MB) was recounted due to a peak shift. The recount is reported. Sample 1202974876 (RIN 2W3 ) was recounted due to a suspected false positive. The recount is reported. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Manual Integration No manual integrations were performed on data in this batch Additional Comments Additional comments were not required for this sample set Qualifier Information Manual qualifiers were not required Method/Analysis Information Product: Alphaspec Th, Solid Analytical Method DOE EML HASL-300, Th-01-RC Modified Page 25 of 82 Prep Method Analytical Batch Number1 Prep Batch Number Dry Soil Prep 1341979 1341955 Sample ID Client ID 336330001 3-4N6 5-7 336330002 3-4N 8-9 336330003 3-4N 10 5-11 336330004 2W4 5-6 336330005 2W4 8-9 336330006 2W4 11-12 336330007 2W4 16-17 336330008 2W4 13 5-14.5 336330009 2W3 6-7 336330010 2W3 7 5-8 5 336330011 2W3 9 5-10.5 336330012 2W3 13-14 336330013 2E1-5.5-6.5 336330014 2E1-12-13 336330015 2E1-17-18 336330016 2E1-23-24 336330017 2E1-26-27 336330018 3-6N 5-6 336330019 3-6N 9-9.5 336330020 3-6N 13-14 1202974964 Method Blank (MB) 1202974965 33633000K3-4N 6 5-7) Sample Duplicate (DUP) 1202974966 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-038 REV# 16. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Page 26 of 82 Qualify Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch Designated QC The following sample was used for QC. 336330001 (3-4N 6.5-7). QC Information All of the QC samples met the required acceptance limits. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Manual Integration Manual integration of alpha spectroscopy spectra 336330005 (2W4 8-9) was performed to fully separate counts in Regions of Interest which would have been biased. Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required Method/Analysis Information Product: Alphaspec U, Solid Analytical Method DOE EML HASL-300, U-02-RC Modified Prep Method. Dry Soil Prep Analytical Batch Number. 1341980 Prep Batch Number. 1341955 Sample ID Client ID 336330001 3-4N 6.5-7 336330002 3-4N 8-9 Page 27 of 82 336330003 3-4N 10 5-11 336330004 2W4 5-6 336330005 2W4 8-9 336330006 2W4 11-12 336330007 2W4 16-17 336330008 2W4 13 5-14 5 336330009 2W3 6-7 336330010 2W3 7 5-8.5 336330011 2W3 9.5-10 5 336330012 2W3 13-14 336330013 2E1-5.5-6.5 336330014 2E1-12-13 336330015 2E1-17-18 336330016 2E1-23-24 336330017 2E1-26-27 336330018 3-6N 5-6 336330019 3-6N 9-9.5 336330020 3-6N 13-14 1202974967 Method Blank (MB) 1202974968 336330001(3-4N 6.5-7) Sample Duplicate (DUP) 1202974969 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-011 RJEV# 24. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch Designated QC The following sample was used for QC. 336330001 (3-4N 6.5-7). QC Information All of the QC samples met the required acceptance limits Page 28 of 82 Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis Sample 336330010 (2W3 7.5-8.5) was recounted due to a peak shift. The recount is reported. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents The following DER was generated for this SDG. DER 1240944 was generated due to Peak Centroid Values Off 1 The U-232 tracer for sample 336330010 is greater than 50 keV from the expected energy of 5302 keV 1. The tracer peak is within the U-232 ROl and the tracer recovery does meet the acceptance criteria. Reporting results. Manual Integration Manual integration of alpha spectroscopy spectra 336330010 (2W3 7.5-8.5) was performed to fully separate counts in Regions of Interest which would have been biased Additional Comments Additional comments were not required for this sample set Qualifier Information Manual qualifiers were not required Method/Analysis Information Product: Alphaspec Th, Solid Analytical Method. DOE EML HASL-300, Th-01-RC Modified Prep Method: Dry Soil Prep Analytical Batch Number. 1342000 Prep Batch Number 1341956 Sample ID 336330021 336330022 336330023 336330024 336330025 336330026 336330027 336330028 336330029 336330030 Client ID 3-6N 13-14D 3-6N 16-17.5 2W2 7-8 2W2 11 5-13 5 2W2 11 5-13.5D 2W2 16.5-17.5 2W6-S(2) 11 5-12 2W6-S(2) 12.5-13 2W6-S(3) 14.5-15 2W6-S(3) 16-17 Page 29 of 82 336330031 1202975002 1202975003 1202975004 2W6-S(2) 14-14 5 Method Blank (MB) 336330022(3-6N 16-17.5) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-038 REV# 16 Calibration Information: Calibration Information All initial and continuing calibration requirements have been met Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC 336330022 (3-6N 16-17 5). QC Information All of the QC samples met the required acceptance limits Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time Sample Re-prep/Re-analysis Sample 336330031 (2W6-S(2) 14-14 5) was recounted due to high carrier/tracer yield. The recount is reported. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Manual Integration No manual integrations were performed on data in this batch Additional Comments Additional comments were not required for this sample set Page 30 of 82 Qualifier Information Manual qualifiers were not required. Method/Analysis Information Product: Alphaspec U, Solid Analytical Method: DOE EML HASL-300, U-02-RC Modified Prep Method: Dry Soil Prep Analytical Batch Number 1342001 Prep Batch Number. 1341956 Sample ID Client ID 336330021 3-6N 13-14D 336330022 3-6N 16-17.5 336330023 2W2 7-8 336330024 2W2 11 5-13.5 336330025 2W2 11.5-13.5D 336330026 2W2 16.5-17.5 336330027 2W6-S(2) 11.5-12 336330028 2W6-S(2) 12.5-13 336330029 2W6-S(3) 14.5-15 336330030 2W6-S(3) 16-17 336330031 2W6-S(2) 14-14.5 1202975005 Method Blank (MB) 1202975006 336330022(3-6N 16-175) Sample Duplicate (DUP) 1202975007 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP) The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-011 REV# 24. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Page 31 of 82 Quality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch Designated QC The following sample was used for QC 336330022 (3-6N 16-17.5). QC Information All of the QC samples met the required acceptance limits Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis Samples 336330029 (2W6-S(3) 14.5-15) and 336330030 (2W6-S(3) 16-17) were recounted due to detector error. The recounts are reported Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG Manual Integration No manual integrations were performed on data in this batch. Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required. Method/Analysis Information Product: Analytical Method: Prep Method: Analytical Batch Number: Prep Batch Number: GFPC, Pt>210, Solid DOE RP280 Modified Dry Soil Prep 1342067 1341955 Sample ID Client ID 336330001 3-4N6 5-7 336330002 3-4N 8-9 336330003 3-4N10 5-11 336330004 2W4 5-6 336330005 2W4 8-9 336330006 2W4 11-12 336330007 2W4 16-17 336330008 2W4 13 5-14 5 336330009 2W3 6-7 336330010 2W3 7.5-8 5 336330011 2W3 9 5-10 5 336330012 2W3 13-14 336330013 2E1-5 5-6.5 336330014 2E1-12-I3 336330015 2E1-17-18 336330016 2E1-23-24 336330017 2E1-26-27 336330018 3-6N 5-6 1202975221 Method Blank (MB) 1202975222 336330004(2W4 5-6) Sample Duplicate (DUP) 1202975223 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-018 REV# 13. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates Sample Geometry All counting sources were prepared in the same geometry as the calibration standards Quality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch Designated QC The following sample was used for QC: 336330004 (2W4 5-6). QC Information All of the QC samples met the required acceptance limits Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time Page 33 of 82 Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents A data exception report (DER) was not generated for this SDG Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required. Method/Analysis Information Product: Analytical Method' Prep Method Analytical Batch Number: Prep Batch Number GFPC, Pb210, Solid DOE RP280 Modified Dry Soil Prep 1342068 1341955 Sample ID Client ID 336330019 3-6N 9-9 5 336330020 3-6N 13-14 336330021 3-6N 13-14D 336330022 3-6N 16-17.5 336330023 2W2 7-8 336330024 2W2 11.5-13 5 336330025 2W2 115-13.5D 336330026 2W2 16 5-17 5 336330027 2W6-S(2) 11 5-12 336330028 2W6-S(2) 12.5-13 336330029 2W6-S(3) 14.5-15 336330030 2W6-S(3) 16-17 336330031 2W6-S(2) 14-14 5 1202981562 Method Blank (MB) 1202981563 336330019(3-6N 9-9 5) Sample Duplicate (DUP) 1202981564 Laboratory Control Sample (LCS) Page 34 of 82 The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-018 REV# 13. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards Quality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch Designated QC The following sample was used for QC: 336330019 (3-6N 9-9.5). QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The blank result 1202981562 (MB) is greater than the MDC but less than the required detection limit. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required. Page 35 of 82 Method/Analvsis Information Product: GFPC, Pb2I0, Liquid Analytical Method. DOE RP280 Modified Analytical Batch Number. 1342069 Sample ID 336330032 336330033 336330034 1202975224 1202975225 1202975226 Client ID RIN 2W3 RIN 3-4N RIN 2W6-S(2) Method Blank (MB) 336330032(RIN 2W3 ) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP) The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-018 REV# 13. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates Sample Geometry All counting sources were prepared in the same geometry as the calibration standards Quality Control (00 Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 336330032 (RIN 2W3 ). QC Information All of the QC samples met the required acceptance limits. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Page 36 of 82 Sample Re-prep/Re-analysis Sample 1202975225 (RIN 2W3 ) was recounted due to a suspected false positive. The recount is reported Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG Additional Comments Additional comments were not required for this sample set Qualifier Information Manual qualifiers were not required. Method/Analysis Information Product: Lucas Cell, DOE Ra-04, Ra226, liquid Analytical Method DOE EML HASL-300 Ra-04 Analytical Batch Number- 1342217 The samples in this SDG were analyzed on an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP) The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-008 REV# 14. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met Standards Information Sample ID 336330032 336330033 336330034 1202975632 1202975633 1202975634 1202975635 Client ID RIN 2W3 RIN 3-4N RIN 2W6-S(2) Method Blank (MB) 336330032(RIN 2W3 ) Sample Duplicate (DUP) 336330032(R1N 2W3 ) Matrix Spike (MS) Laboratory Control Sample (LCS) Page 37 of 82 Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control fOC) Information: Blank Information The blank volume is representative of the sample volume in this batch Designated QC The following sample was used for QC: 336330032 (RIN 2W3 ). QC Information All of the QC samples met the required acceptance limits. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required Method/Analysis Information Product: Lucas Cell, DOE Ra-04, Ra226, solid Analytical Method. DOE EML HASL-300 Ra-04 Prep Method: Dry Soil Prep Analytical Batch Number 1342297 Prep Batch Number 1341955 Sample ID Client ID 336330001 3-4N6 5-7 Page 38 of 82 336330002 3-4N 8-9 336330003 3-4N 10.5-11 336330004 2W4 5-6 336330005 2W4 8-9 336330006 2W4 11-12 336330007 2W4 16-17 336330008 2W4 13 5-14 5 336330009 2W3 6-7 336330010 2W3 7 5-8 5 336330011 2W3 9.5-10 5 336330012 2W3 13-14 336330013 2E1-5.5-6.5 336330014 2E1-12-13 336330015 2E1-17-18 1202975800 Method Blank (MB) 1202975801 336330001(3-4N 6.5-7) Sample Duplicate (DUP) 1202975802 336330001(3-4N 6.5-7) Matrix Spike (MS) 1202975803 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP) The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-008 REV# 14 Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates Sample Geometry All counting sources were prepared in the same geometry as the calibration standards Quality Control fOC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC- 336330001 (3-4N 6.5-7) QC Information All of the QC samples meet the required acceptance limits with the following exceptions The Matrix Spike 1202975802 (3-4N 6 5-7) did not meet recovery requirements due to the sample activity being greater than five times the spiked nominal concentration Technical Information: Holding Time Page 39 of 82 All sample procedures for this sample set were performed within the required holding time Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required Method/Analvsis Information Product: Analytical Method. Prep Method- Analytical Batch Number: Prep Batch Number- Lucas Cell, DOE Ra-04, Ra226, solid DOE EML HASL-300 Ra-04 Dry Soil Prep 1342298 1341955 Sample ID Client ID 336330016 2E1-23-24 336330017 2E1-26-27 336330018 3-6N 5-6 336330019 3-6N 9-9.5 336330020 3-6N 13-14 336330021 3-6N 13-14D 336330022 3-6N16-17 5 336330023 2W2 7-8 336330024 2W2 11 5-13.5 336330025 2W2 115-13 5D 336330026 2W2 16 5-17.5 336330027 2W6-S(2) 11 5-12 336330028 2W6-S(2) 12 5-13 336330029 2W6-S(3) 14 5-15 336330030 2W6-S(3) 16-17 336330031 2W6-S(2) 14-14 5 1202975805 Method Blank (MB) 1202975806 336330016(2E 1-23-24) Sample Duplicate (DUP) 1202975807 336330016(2El-23-24) Matrix Spike (MS) Page 40 of 82 1202975 808 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-008 REV# 14 Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards Quality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch Designated QC The following sample was used for QC: 336330016 (2E1-23-24) QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The Matrix Spike 1202975807 (2E1-23-24) did not meet recovery requirements due to the sample activity being greater than five times the spiked nominal concentration Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG Additional Comments Additional comments were not required for this sample set Qualifier Information Manual qualifiers were not required. Page 41 of 82 Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative Page 42 of 82 Qualifier Definition Report for DNMI001 Energy Fuels Resources (USA), Inc. Client SDG: 336330 GEL Work Order: 336330 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. Review/V alidation GEL requires all analytical data to be verified by a qualified data reviewer In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report. Name: Heather McCarty Date: 13 NOV 2013 Title: Analyst II Page 43 of 82 GEL Laboratories LLC Form GEL-DER DER Report No.. 1240944 Revision No.: 2 DATA EXCEPTION REPORT Mo.Day Yr. 12-NOV-13 Division: Radiochemistry Quality Criteria: Specifications Type: Process Instrument Type: ALPHA SPECTROMETER Test / Method' DOE EML HASL-300, U-02-RC Matrix Type: Solid Client Code: DNMI Modified Batch ID: 1341980 Sample Numbers: see below Potentially affected work order(s)(SDG): 336330 Application Issues: Peak Centroid Values Off Specification and Requirements Exception Description DER Disposition: 1 The U-232 tracer for sample 336330010 is greater than 50 keV from the expected energy of 5302 keV 1 The tracer peak is within the U-232 ROI and the tracer recovery does meet the acceptance criteria Reporting results. Originator's Name: Jessica Downey 12-NOV-13 Data Validator/Group Leader: Jessica Davis 12-NOV-13 Page 44 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company Address . Contact. Project. Certificate of Analysis Report Date November 13, 2013 Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID. Matrix- Collect Date. Receive Date: Collector. 3-4N 6 5-7 336330001 Solid 22-OCT-13 13:10 25-OCT-13 Client Project' Client ID- DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 62 2 Alphaspec U, Solid "Dry Weight Corrected" L'raniuni-238 24 7 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 91 1 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 149 >/-l 73 The following Prep Methods were performed' +/-1 72 +/-] 29 87 0 485 0491 0 822 0 246 1 00 1 00 5 00 1 00 pCi/g pCi/g pCVg pCi.g JXH2 11/11/13 1010 1341979 1 JXH2 11/08/13 1043 13419,80 2 KDF1 1113'13 0833 1342067 3 KSDI 11/12/13 1305 1342297 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: cxci 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300. U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 91 4 91 5 104 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 45 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel com Company Address Contact Project Certificate of Analysis Report Date: November 13, 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID. Matrix Collect Date: Receive Date. Collector' 3-4N 8-9 336330002 Solid 22-OCT-13 13:20 25-OCT-13 Client Project. Client ID DNMI00I07 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 58 4 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 29 4 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 120 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 153 77 The following Prep Methods were performed: +/-1 60 +/-1 40 +1-2 32 0 448 0 368 0 948 0 331 1 00 1 00 5 00 I 00 pCi/g pCi/g pCi/g pCi/g JXH2 11/11/13 1010 1341979 I JXH2 11/08/13 1043 1341980 2 KDFl 11/13/13 0833 1342067 3 KSD1 11/12/13 1305 1342297 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed. CXCl 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300. Th-01-RC Modified DOE EML HASL-300. U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 101 88 9 92 5 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 46 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www gel.com Company Address Contact: Project. Certificate of Analysis Report Date: November 13, 2013 Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID: Sample ID Matrix: Collect Date Receive Date Collector 3-4N 10 5-11 336330003 Solid 22-OCT-13 13:30 25-OCT-13 Client Project' Client ID: DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 120 Alphaspec U, Solid "Dry Weight Corrected" L'raiuum-238 25 7 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 105 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 230 +1-2 24 The following Prep Methods were performed: +1-2 55 +1-1 66 +1-2 08 0 542 I 10 I 03 0 353 I 00 I 00 5 00 1 00 pCi/g pCi/g pCi/g pCi/g JXH2 1111/13 1010 1341979 I JXH2 11/08/13 1043 1341980 2 KDF1 11/13/13 0833 1342067 3 KSD1 11'12/13 1305 1342297 4 Method Description Analyst Date Time Prep Batch Dry Sod Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed. cxci 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOF EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 83 1 61 0 105 (15%-125%) (I5%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit. For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 47 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company : Address Contact- Project. Certificate of Analysis Report Date. November 13, 2013 Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID. Matrix- Collect Date Receive Date. Collector. 2W4 5-6 336330004 Solid 21-OCT-13 15:25 25-OCT-13 Client Project- Client ID DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 200 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 22 9 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 362 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 385 +/-2 83 The following Prep Methods were performed• +/-3 35 +/-1 20 t/-3 90 0 550 0 300 I 03 0 336 1 00 1 00 5 00 1 00 pCi/g pCi/g pCig pCi/g JXH2 11/11/13 1010 1341979 1 JXH2 11/08/13 1043 1341980 2 KDF1 11-13/13 0833 1342067 3 KSDI 11,12 13 1305 1342297 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed cxci 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 87 1 105 98 5 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Page 48 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel com Certificate of Analysis Report Date. November 13, 2013 Company . Address Contact- Project. Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Tailings Soil Characterization Client Sample ID: Sample ID Matrix- Collect Date- Receive Date. Collector 2W4 8-9 336330005 Solid 21-OCT-13 15:30 25-OCT-13 Client Project: Client ID: DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 708 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 47 4 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 485 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 749 +/-3 71 The following Prep Methods were performed +/-5 09 +/-2 11 +/-5 16 0 398 0 519 1 23 0 226 I 00 I 00 5 00 I 00 Pd'g pCi/g Pd'g pCi'g JXH2 i I JI /J 3 1010 1341979 1 JXH2 11/08/13 1043 1341980 2 KDF1 11 13'13 0833 1342067 3 KSDI III2'I3 1305 1342297 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: cxci 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC. Pb210, Solid "Dry Weight Corrected" 121 74 2 75 3 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 49 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 13, 2013 Company Address : Contact. Project. Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID Matrix: Collect Date Receive Date: Collector. 2W4 11-12 336330006 Solid 21-OCT-13 25-OCT-13 Client Project- Client ID DNMI00I07 DNMI00I 15-40 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 525 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 146 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 555 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 678 +/-3 54 The following Prep Methods were performed- +/-4 74 +/-3 40 +/-6.30 0 463 0 380 1 99 0 299 1 00 1 00 5 00 1 00 pCi/g pCi/g pCi/g pCi/g JXH2 11/11/13 1010 1341979 1 JXH2 11/08/13 1043 1341980 2 KDFl 11/13/13 0833 1342067 3 KSD1 11/12/13 1340 1342297 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed- CXCl 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300. Th-01-RC Modified DOfc EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb2IO, Solid "Dry Weight Corrected" 118 75 6 58 8 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit. For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 50 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www gel.com Company Address . Contact Project. Certificate of Analysis Report Date November 13, 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID Matrix. Collect Date: Receive Date. Collector 2W4 16-17 336330007 Solid 21-OCT-13 16.00 25-OCT-13 Client Project- Client ID- DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 514 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 46 3 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weigr t Corrected" Lead-210 960 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226 solid "Dry Weight Corrected" Radium-226 826 +/-3 94 The following Prep Methods wtre performed. Method +/-4 77 +/-1 66 +/-8 07 0 469 0 329 1 37 0 304 1 00 1 00 5 00 I 00 pCi/g pCi/g pCi/g pCi/g JXH2 ll/ll'13 1010 1341979 1 JXH2 11/08/13 1043 1341980 2 KDFl 1 113/13 0833 1342067 3 KSD1 11/12/13 1340 1342297 4 Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed. CXCI 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC. Pb210, Solid "Dry Weight Corrected" 124 100 62 8 (15%-125%) (15%-125%) (25%-125%) Notes: 1 Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 51 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company , Address . Contact. Project Certificate of Analysis Report Date: November 13, 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID Sample ID. Matrix Collect Date Receive Date. Collector. 2W4 13 5-14 5 336330008 Solid 21-OCT-13 25-OCT-13 Client Project Client ID DNM100107 DNMI001 5:50 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 493 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 23 7 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 653 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 735 +/-4I5 The following Prep Methods were performed- H-4 64 +/-1 23 +/-6 00 0 668 0 354 I 51 0 288 1 00 1 00 5 00 00 pCi/g pCi/g pCi/g pCi/g JXH2 11/11/13 1010 1341979 I JXH2 11/08/13 1043 1341980 2 KDFl 11/13/13 0833 1342067 3 KSD1 1L12'13 1340 1342297 4 Method Description Analyst Dale Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: CXCl 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC. Pb2IO. Solid "Dry Weight Corrected" 115 99 2 74 7 (15%-125%) (15%-125%) (25%-l25%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 52 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 13,2013 Company Address . Contact: Project: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID: Matrix. Collect Date. Receive Date: Collector 2W3 6-7 336330009 Solid 21-OCT-13 16:35 25-OCT-13 Client Project: Client ID- DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 554 +/-5 05 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 62 0 +/-2 04 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 858 W-8 08 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 946 +/-4 29 The following Prep Methods were performed. 0 557 0 372 2 33 0 314 I 00 1 00 5 00 1 00 pCi/g pCi/g pCi/g pCi/g JXH2 11/11 13 1010 1341979 I JXH2 11/08/13 1043 1341980 2 KDFl 11/13/13 0833 1342067 3 KSD1 11/12/13 1340 1342297 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: CXCl 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC. Pb2IO, Solid "Dry Weight Corrected" 108 99 3 56 2 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 53 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel com Certificate of Analysis Report Date. November 13, 2013 Company . Address Contact. Project Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID. Matrix. Collect Date- Receive Date- Collector 2W3 7 5-8 5 336330010 Solid 21-OCT-13 If 25-OCT-I3 Client Project: Client ID DNM100107 DNMI001 •40 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 448 +/-3 86 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 98 7 +/-3 83 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 980 +/-8 23 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 482 +/-3 35 The following Prep Methods were performed: 0 373 0 446 271 0 287 1 00 1 00 5 00 1 00 pCi/g pCi/g pCi/g pCi/g JXH2 11/11/13 1010 1341979 1 JXH2 11/11/13 1305 1341980 2 KDFl 11/13/13 0833 1342067 3 KSD1 11/12/13 1340 1342297 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: Method CXCl 10/25/13 1402 1341955 Description Analyst Comments DOE EML HASL-300. Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th. Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb2l0, Solid "Dry Weight Corrected" 115 46 9 55 5 (15%-125%) (15%-12 5%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 54 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www gel.com Company . Address . Contact. Project. Certificate of Analysis Report Date: November 13, 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID Sample ID. Matrix. Collect Date: Receive Date. Collector: 2W3 9 5-10.5 336330011 Solid 21-OCT-13 1655 25-OCT-13 Client Project Client ID. DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 428 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 35 8 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 884 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 635 +/-3 66 The following Prep Methods were performed. +/-4 20 +/-1 59 +/-6 30 0 456 0211 1 57 0 341 1 00 1 00 5 00 1 00 pCi/g pCi/g pCVg pCi'g JXH2 H'll/13 1010 1341979 I JXH2 II'08/13 1043 1341980 2 KDFl 11/13/13 0833 1342067 3 KSD1 11 .12/13 1340 1342297 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed. cxci 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 106 106 93 9 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit. For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 55 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company Address . Contact Project Certificate of Analysis Report Date: November 13, 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID Sample ID Matrix. Collect Date- Receive Date Collector: 2W3 13-14 336330012 Solid 21-OCT-13 25-OCT-13 Client Project- Client ID- DNMI00107 DNMI001 17:05 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 176 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 9 79 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 133 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 166 73 The following Prep Methods were performed +1-2 87 +1-0 778 +1-2 24 0 509 0 294 0 856 0291 1 00 I 00 5 00 1 00 pCi/g pCi/g pCi/g pCi/g JXH2 11/11/13 1010 1341979 1 JXH2 11/08/13 1043 1341980 2 KDFl 11/13/13 0833 1342067 3 KSD1 11/12/13 1410 1342297 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed. CXCI 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300. Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210. Solid "Dry Weight Corrected" 95 6 109 106 (I5%-125%) (I5%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Page 56 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company : Address . Contact: Project. Certificate of Analysis Report Date. November 13, 2013 Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID: Matrix' Collect Date. Receive Date Collector' 2E1-5.5-6 5 336330013 Solid 21-OCT-13 14:00 25-OCT-I3 Client Project' Client ID: DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 124 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 6 39 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 234 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 294 U-2 35 The following Prep Methods were performed' +/-2 45 +/-0 656 W-3 39 0 513 0 367 I 05 0 303 I 00 1 00 5 00 1 00 pCi'g pCi/g pCi'g PCi'g JXH2 11/11/13 1010 1341979 I JXH2 11/08/13 1043 1341980 2 KDFl 11/13/13 0833 1342067 3 KSD1 11'12/13 1410 1342297 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed' cxci 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 100 98 9 81 3 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit. For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 57 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www gel.com Company . Address . Contact. Project. Certificate of Analysis Report Date: November 13, 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID Sample ID Matrix. Collect Date: Receive Date Collector 2E1-12-13 336330014 Solid 21-OCT-13 25-OCT-13 Client Project: Client ID- DNMI00107 DNMI001 4.10 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 295 +/-3 57 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 14 0 +/-1 01 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 458 +/-4 16 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 656 +/-3 64 The following Prep Methods were performed' 0 462 0 346 0 781 0 249 1 00 1 00 5 00 1 00 pC./g pCi/g pCi/g pCi/g JXH2 11/11/13 1010 1341979 1 JXH2 11/08/13 1043 1341980 2 KDFl 11/13/13 0833 1342067 3 KSD1 11/12/13 1410 1342297 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed CXCl 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOF EML HASL-300. U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th. Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 99 9 97 7 104 (I5%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 58 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel com Company Address : Contact. Project. Certificate of Analysis Report Dale: November 13, 2013 Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Tailings Soil Characterization Client Sample ID: Sample ID. Matrix. Collect Date- Receive Date Collector 2E1-17-18 336330015 Solid 21-OCT-13 14:20 25-OCT-13 Client Project. Client ID- DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 199 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 13 8 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 320 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 531 +/-3 53 The following Prep Methods were performed +/-3 05 +/-0 963 +/-3 73 0 512 0319 0 875 0 380 1 00 1 00 5 00 1 00 pCi/g pCi/g pCi/g pCi'g JXH2 1 1/1113 1010 1341979 I JXH2 11/08/13 1043 1341980 2 KDFl 11-13/13 0833 1342067 3 KSD1 1112/13 1410 1342297 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed CXCl 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300. Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 103 100 87 2 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Page 59 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company Address • Contact. Project. Certificate of Analysis Report Date: November 13, 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID. Matrix: Collect Date- Receive Date. Collector- 2E1-23-24 336330016 Solid 21-OCT-13 14:35 25-OCT-13 Client Project: Client ID DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 122 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 16 6 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 100 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 146 +/-1 95 The following Prep Methods were performed +/-2 30 +/-1 08 +/-1 94 0 489 0 383 0 758 0 421 1 00 1 00 5 00 1 00 PCi'g pCi/g pCi/g pCi/g JXH2 11/11/13 1010 1341979 1 JXH2 11/08/13 1043 1341980 2 KDFl 11/13/13 0833 1342067 3 KSD1 11/09/13 1625 1342298 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed CXCI 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300. Th-01-RC Modified DOE EML HASL-300. U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th. Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC. Pb210, Solid "Dry Weight Corrected" 90 5 90 2 106 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 60 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company . Address : Contact. Project. Certificate of Analysis Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Report Date. November 13, 2013 Client Sample ID. Sample ID. Matrix Collect Date: Receive Date. Collector 2E1-26-27 336330017 Solid 21-OCT-13 14:50 25-OCT-13 Client Project: Client ID- DNM100107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 142 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 15 3 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 249 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 328 +/-2 97 0 434 The following Prep Methods were performed. +/-2 64 +/-1 06 +/-3 13 0 517 0 447 1 09 1.00 1 00 5 00 1 00 pCi'g pCi/g pCi/g pCi/g JXH2 11/11/13 1010 1341979 I JXH2 11 '08/13 1043 1341980 2 KDFl 11/13/13 0833 1342067 3 KSD1 1 1/09/13 1700 1342298 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: CXCl 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300. Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uramum-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC. Pb210, Solid "Dry Weight Corrected" 84 1 96 3 101 (I5%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit. For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Page 61 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel com Certificate of Analysis Report Date: November 13, 2013 Company . Address ' Contact. Project: Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Tailings Soil Characterization Client Sample ID Sample ID: Matrix. Collect Date Receive Date: Collector. 3-6N 5-6 336330018 Solid 22-OCT-13 10:50 25-OCT-13 Client Project: Client ID: DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 117 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 21 7 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 139 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 178 +/-2 12 The following Prep Methods were performed: + 1-2 36 +/-1 82 +1-2 73 0 490 0 839 I 08 0 407 I 00 1 00 5 00 1 00 pCi.g pCi/g pCi'g pCi/g JXH2 11/11/13 1010 1341979 1 JXH2 11/08/13 1043 1341980 2 KDFl 11/13/13 0848 1342067 3 KSD1 11/09/13 1700 1342298 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed CXCl 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 77 1 43 6 98 5 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Page 62 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company : Address . Contact. Project. Certificate of Analysis Report Dale November 13, 2013 Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Tailings Soil Characterization Client Sample ID: Sample ID Matrix- Collect Date: Receive Date: Collector 3-6N 9-9 5 336330019 Solid 22-OCT-13 11 05 25-OCT-13 Client Project: Client ID. DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 2240 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected Radium-226 243 The following Prep Methods were performed: 148 238 1/-9 28 0 450 t/-3 59 0 533 *7-3 34 +/-2 79 I 38 0 517 I 00 I 00 5 00 1 00 pCi g pCi/g pCi/g pCi/g JXH2 II 11/13 1010 1341979 1 JXH2 11-08'13 1044 1341980 2 KDFl 11/13/13 0924 1342068 KSD1 11/09/13 1700 1342298 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: CXCi 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 109 71 0 84 6 (15%-125%) (I5%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 63 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: November 13, 2013 Company Address : Contact Project: Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID' Sample ID' Matrix. Collect Date Receive Date. Collector 3-6N 13-14 336330020 Solid 22-OCT-13 25-OCT-13 Client Project: Client ID- DNMI00I07 DNMI001 1.20 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 1390 +/-8 58 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 262 +1-5 54 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 1390 +1-150 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 1670 +1-1 20 The following Prep Methods were performed- 0 589 0 560 1 31 0 500 1 00 1 00 5 00 1 00 pCi/g pCi/g PCi/g pCi/g JXH2 11/11/13 1010 1341979 I JXH2 11/08/13 1044 1341980 2 KDFl 11/13/13 0925 1342068 3 KSD1 11/09/13 1700 1342298 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed- cxci 10/25/13 1402 1341955 Method Description Analyst Comments DOE EML HASL-300. Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb2l0. Solid "Dry Weight Corrected" 87 5 61 9 105 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 64 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company . Address Contact Project. Certificate of Analysis Report Date November 13. 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID: Sample ID. Matrix- Collect Date- Receive Date. Collector- 3-6N 13-14D 336330021 Solid 22-OCT-13 11:20 25-OCT-13 Client Project: Client ID DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 930 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 251 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 1360 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 1310 +/-5 98 The following Prep Methods were performed- +/-6 75 +/-5 52 +/-7 09 0 539 0 741 1 15 0 442 1 00 1 00 5 00 1 00 pCi/g pCi/g pCi/g pCi'g HAKB 11/08'13 1255 1342000 1 HAKB 11.09'13 1135 1342001 2 KDFl 11/13/13 0927 1342068 3 KSDI 1109'13 1700 1342298 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: CXCl 10/25/13 1406 1341956 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 114 59 5 106 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Page 65 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date. November 13, 2013 Company : Address . Contact: Project' Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Tailings Soil Characterization Client Sample ID- Sample ID: Matrix Collect Date- Receive Date. Collector. 3-6N 16-17 5 336330022 Solid 22-OCT-13 11 25-OCT-13 Client Project. Client ID. DNMI00107 DNMI00I .30 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 859 +1-6 54 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 185 +/-4 54 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 1230 +/-6 63 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 1480 +/-6 62 The following Prep Methods were performed' o 509 0 534 1 24 0 427 1 00 1 00 5 00 1 00 pCi/g pCi/g pCi/g pCi/g HAKB 11/08/13 1255 1342000 1 HAKB 11/09/13 1135 1342001 2 KDFl 11/13/13 0927 1342068 3 KSD1 11/09/13 1700 1342298 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed cxci 10/25/13 1406 1341956 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC. Pb2l0, Solid "Dry Weight Corrected" 120 65 8 105 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Page 66 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company • Address . Contact. Project. Certificate of Analysis Report Dale November 13, 2013 Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID. Matrix: Collect Date: Receive Date: Collector: 2W2 7-8 336330023 Solid 22-OCT-13 09:20 25-OCT-13 Client Project: Client ID- DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 728 +/-5 97 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 75 I +/-2 27 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 1050 +/-6 12 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 913 +/-4 72 The following Prep Methods were performed 0 513 0417 1 03 0 394 1 00 1 00 5 00 1 00 pCi'g pCi/g pCi/g pCi/g HAKB 1 1/08/13 1255 1342000 I HAKB 11/09/13 1135 1342001 2 KDFl 11/13/13 0927 1342068 KSD1 11/09'13 1730 1342298 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed. cxci 10/25/13 1406 1341956 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 117 102 108 (15%-125%) (I5%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 67 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company Address . Contact Project. Certificate of Analysis Report Date November 13, 2013 Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID. Matrix Collect Date. Receive Date. Collector 2W2 115-135 336330024 Solid 22-OCT-13 08:35 25-OCT-13 Client Project. Client ID DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 290 +/-4 21 Alphaspec U. Solid "Dry Weight Corrected" Uraruum-238 15 3 +/-1 19 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 200 +/-2 61 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 107 +/-1 60 The following Prep Methods were performed' 0 635 0 439 1 II 0 384 1 00 I 00 5 00 1 00 pCi/g pCi/g pCi/g pCi/g HAKB 11/08/13 1255 1342000 1 HAKB 11/09/13 1135 1342001 2 KDFl 11/13/13 0936 1342068 3 KSD1 1 1/09/13 1730 1342298 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed. CXCI 10/25/13 1406 1341956 Method Description Analyst Comments DOE EML HASL-300. Th-01-RC Modified DOE EML HASL-300. U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb2IO, Solid "Dry Weight Corrected" 103 80 8 107 (15%-125%) (15%-I25%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Page 68 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company Address : Contact Project. Certificate of Analysis Report Date: November 13, 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID: Sample ID. Matrix. Collect Date- Receive Date. Collector 2W2 11.5-13.5D 336330025 Solid 22-OCT-13 08:35 25-OCT-13 Client Project- Client ID DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 427 +/-4 85 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 44 2 85 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 740 +/-6.15 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 553 +/-4 04 0 476 The following Prep Methods were performed1 0 543 0 472 1 55 1 00 I 00 5 00 1 00 pCi/g pCi/g pCi/g pCi/g HAKB 11/08/13 1255 1342000 I HAKB 11/09/13 1135 1342001 2 KDFl 11/13/13 0936 1342068 3 KSD1 11.'09/13 1730 1342298 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: cxci 10/25/13 1406 1341956 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb2l0, Solid "Dry Weight Corrected" 118 105 77 3 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Page 69 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 13, 2013 Company : Address . Contact Project Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID Sample ID Matrix: Collect Date. Receive Date Collector: 2W2 16 5-17 5 336330026 Solid 22-OCT-13 08:55 25-OCT-13 Client Project- Client ID- DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 349 +/-4 11 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 419 85 Rad Gas Flow Proportional Counting GFPC, Pb2IO, Solid "Dry Weight Corrected" Lead-210 675 +/-5 15 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 648 +/-4 54 The following Prep Methods were performed 0 663 0 539 I 14 0 515 1 00 1 00 5 00 1 00 pCi/g pCi/g pCi/g Pt-'i'g HAKB 11/08/13 1255 1342000 I HAKB 11/09/13 1135 1342001 2 KDFl 11/13/13 0937 1342068 3 KSD1 11/09/13 1730 1342298 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed. CXCl 10/25/13 1406 1341956 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300. U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thoriuin-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Conected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 124 100 97 8 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 70 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company ; Address Contact Project: Certificate of Analysis Report Date November 13, 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID. Matrix: Collect Date. Receive Date Collector: 2W6-S(2) 11 5-12 336330027 Solid 23-OCT-13 10:00 25-OCT-13 Client Project: Client ID. DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 607 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 24 9 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 1040 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 1240 +/-6 04 The following Prep Methods were performed' U-b 49 +/-I 36 +/-6 04 0 658 0 354 I 09 0 474 1 00 I 00 5 00 1 00 pCi.g pCi/g pCi/g pCi/g HAKB 11 08' 13 1255 1342000 I HAKB 11/09']3 1 135 1342001 2 KDFl 11/13/13 0937 1342068 3 KSD1 11'09/13 1730 1342298 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed CXCl 10/25/13 1406 1341956 Method I 2 3 4 Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb2l0, Solid "Dry Weight Corrected" 80 0 98 1 108 (15%-125%) (I5%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 71 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company Address . Contact. Project Certificate of Analysis Report Date. November 13, 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID Matrix. Collect Date- Receive Date. Collector 2W6-S(2) 12 5-13 336330028 Solid 23-OCT-13 10:10 25-OCT-13 Client Project: Client ID- DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 219 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 56 2 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 204 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 276 +1-2 75 The following Prep Methods were performed- 17-3 54 +1-2 04 +1-2 78 0 701 0 409 I 01 0 441 1 00 I 00 5 00 1 00 pCi/g pCi/g pCi/g pCi/g HAKB 11/08/13 1255 1342000 1 HAKB 11/09/13 1135 1342001 2 KDFl 11/13/13 0939 1342068 3 KSD1 11/09/13 1730 1342298 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: CXCl 10/25/13 1406 1341956 Method Description Analyst Comments DOE EML HASL-300. Th-01-RC Modified DOE EML HASL-300. U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC, Pb210, Solid "Dry Weight Corrected" 101 97 7 104 (I5%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 72 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel com Certificate of Analysis Report Date. November 13, 2013 Company : Address • Contact. Project. Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID: Sample ID. Matrix. Collect Date. Receive Date. Collector 2W6-S(3) 14 5-15 336330029 Solid 23-OCT-13 09.05 25-OCT-13 Client Project: Client ID: DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 706 Alphaspec U, Solid "Dry Weight Corrected" Uramum-238 54 0 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 900 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 623 W-4 24 0 356 The following Prep Methods were performed +/-7 46 +/-I 99 + /-5 56 0 699 0219 0 991 1 00 1 00 5 00 1 00 pCi/g pCi'g pCi/g pCi.g HAKB 11/08/13 1201 1342000 1 HAKB 11/11/13 1305 1342001 2 KDFl 11/13/13 0939 1342068 3 KSD1 1L09/13 1805 1342298 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: CXCl 10/25/13 1406 1341956 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Camer Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC. Pb210, Solid "Dry Weight Corrected" 88 0 93 3 110 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Page 73 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel com Company Address Contact. Project. Certificate of Analysis Report Date. November 13, 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID. Matrix: Collect Date- Receive Date Collector 2W6-S(3) 16-17 336330030 Solid 23-OCT-13 09:25 25-OCT-13 Client Project: Client ID- DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 473 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 50 8 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 576 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, solid "Dry Weight Corrected" Radium-226 505 +/-3 39 0 368 The following Prep Methods were performed +/-5 69 +/-2 05 +/-4 38 0 651 0 456 0719 1 00 1 00 5 00 1 00 pCi/g pCi/g PCi/g pd'g HAKB 11/08/13 1201 1342000 I HAKB 11/11/13 1305 1342001 2 KDFl 11/13/13 0944 1342068 3 KSD1 11/09/13 1805 1342298 4 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: CXCl 10/25/13 1406 1341956 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Corrected" Alphaspec U, Solid "Dry Weight Corrected" GFPC. Pb210, Solid "Dry Weight Corrected" 104 81 1 116 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Page 74 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company : Address . Contact. Project. Certificate of Analysis Report Date. November 13, 2013 Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID. Matrix: Collect Date: Receive Date. Collector 2W6-S(2) 14-14.5 336330031 Solid 23-OCT-13 10:30 25-OCT-13 Client Project: Client ID. DNM100107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Solid "Dry Weight Corrected" Thonum-230 646 +1-9 88 1 23 Alphaspec U, Solid "Dry Weight Corrected" Uranium-238 123 +/-3 11 0 480 Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "Dry Weight Corrected" Lead-210 1360 +1-147 0 874 Rad Radium-226 Lucas Cell, DOE Ra-04. Ra226, solid "Dry Weight Corrected" Radium-226 1150 +1-5 45 0 417 The following Prep Methods were performed: i oo 1 oo 5 00 1 00 pCi/g pCi/g pcvg pCi/g HAKB 11.1 1/13 1305 1342000 1 HAKB 11/09/13 1135 1342001 2 KDFl 11/13/13 0944 1342068 KSD1 1109'13 1805 1342298 Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed. cxci 10/25/13 1406 1341956 Method Description Analyst Comments DOE EML HASL-300. Th-01-RC Modified DOE EML HASL-300. U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Solid "Dry Weight Conected" Alphaspec U, Solid "Dry Weight Corrected" GFPC. Pb2IO, Solid "Dry Weight Corrected" 114 92 2 99 8 (15%-125%) (15%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 75 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www gel.com Company . Address • Contact. Project. Certificate of Analysis Report Date: November 13, 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Tailings Soil Characterization Client Sample ID. Sample ID Matrix- Collect Date. Receive Date. Collector RIN 2W3 336330032 Water 21-OCT-13 15:15 25-OCT-13 Client Project. Client ID: DNM100107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Liquid "As Received" Thonum-230 U 0 498 +/-0 222 Alphaspec U, Liquid "As Received" Uranium-238 U 0 533 +/-0 293 Rad Gas Flow Proportional Counting GFPC, Pb210, Liquid "As Received" Lead-210 U 3 09 +/-1 29 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, liquid "As Received" Radium-226 U 0 268 +/-0 117 The following Analytical Methods were performed: 0 596 0 654 3 98 0 351 I 00 I 00 5 00 I 00 pCi/L pCi/L pCi/L pCi/L NXP2 11/06/13 1001 1341943 1 NXP2 11/06/13 0958 1341944 2 KDFl 11/12/13 1422 1342069 3 KSD1 11/06/13 1235 1342217 4 Method Description Analyst Comments DOE EML HASL-300. Th-01-RC Modified DOE EML HASL-300. U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thorium-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Liquid "As Received" Alphaspec U, Liquid "As Received" GFPC, Pb2IO. Liquid "As Received" 85 5 63 0 100 (15%-125%) (I5%-I25%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 76 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www gel.com Company . Address Contact. Project. Certificate of Analysis Report Date November 13, 2013 Energy Fuels Resources (USA), Inc 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID: Sample ID: Matrix: Collect Date- Receive Date: Collector. RIN 3-4N 336330033 Water 22-OCT-13 13:00 25-OCT-13 Client Project: Client ID. DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Liquid "As Received" Thonum-230 U Alphaspec U, Liquid "As Received" Uranium-238 U Rad Gas Flow Proportional Counting GFPC, Pb210, Liquid "As Received" Lead-210 U Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, liquid "As Received" Radium-226 U 0 0971 + /-0 109 The following Analytical Methods were performed. 0 588 -0 0531 1 04 +/-0 250 +/-0 120 17-1 23 0 651 0613 4 36 0 392 1 00 1 00 5 00 1 00 pCi/L pCi/L pCi/L pCi'L NXP2 H'06/13 1001 1341943 1 NXP2 11/06/13 0958 1341944 2 KDFl 11/12/13 1430 1342069 3 KSD1 11/06/13 1235 1342217 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thonum-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Liquid "As Received" Alphaspec U. Liquid "As Received" GFPC, Pb210, Liquid "As Received" 78 7 66 4 109 (I5%-I25%) (I5%-125%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL Page 77 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel com Company Address : Contact. Project. Certificate of Analysis Report Date. November 13, 2013 Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms Kathy Weinel Tailings Soil Characterization Client Sample ID- Sample ID: Matrix. Collect Date: Receive Date. Collector- RIN 2W6-S(2) 336330034 Water 23-OCT-13 10:50 25-OCT-13 Client Project- Client ID- DNMI00107 DNMI001 Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Th, Liquid "As Received" Thorium-230 U 0 321 +/-0 206 Alphaspec U, Liquid "As Received" Uranium-238 U -0 0506 +7-0 114 Rad Gas Flow Proportional Counting GFPC, Pb2I0, Liquid "As Received" Lead-210 U -0 328 +/-0 908 Rad Radium-226 Lucas Cell, DOE Ra-04, Ra226, liquid "As Received" Radium-226 U 0 162 +/-0 101 The following Analytical Methods were performed. 0615 0 584 3 62 0 332 1 00 1 00 5 00 1 00 pCi/L pCi/L pCi/L pCi/L NXP2 11/06/13 1001 1341943 1 NXP2 11/06/13 0958 1341944 2 K.DFI 11/12/13 1423 1342069 3 KSD1 11/06/13 1235 1342217 4 Method Description Analyst Comments DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, U-02-RC Modified DOE RP280 Modified DOE EML HASL-300 Ra-04 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Thormm-229 Tracer Uranium-232 Tracer Lead Carrier Alphaspec Th, Liquid "As Received" Alphaspec U, Liquid "As Received" GFPC, Pb2IO, Liquid "As Received" 78 0 66 4 108 (15%-125%) (15%-I25%) (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma) SRL = Sample Reporting Limit. For metals analysis only When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Page 78 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Contact: Workorder: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Ms. Kathy Weinel 336330 Report Date: November 13, 2013 Page 1 of 4 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1341943 QC 1202974873 336330032 DUP Thonum-230 QC 1202974874 LCS Thonum-230 QC 1202974872 Thonum-230 MB Batch 1341944 QC 1202974876 336330032 DUP Uranium-238 QC 1202974877 LCS Uranium-238 QC 1202974875 MB Uranium-238 Batch 1341979 QC1202974965 336330001 DUP Thonum-230 QC 1202974966 LCS Thonum-230 QC 1202974964 MB Thonum-230 Batch 1341980 QC1202974968 336330001 DUP Uranium-238 QC 1202974969 LCS Uranium-238 QC 1202974967 MB Uraniutn-238 Batch 1342000 QC 1202975003 336330022 DUP Thonum-230 U 0 498 U 0 534 pCi/L N/A Uncertainty +/-0 222 +/-0 268 21.4 22 5 pCt/L Uncertainty +/-1.19 U 0 443 pCi/L Uncertainty +/-0 249 N/A NXP2 11/06/13 10 01 105 (75%-125%) 11/06/13 10 01 11/06/13 10.01 U Uncertainty 27.0 Uncertainty Uncertainty 0 533 U +/-0 293 0 352 pCt/L N/A -/-0 245 25.8 pCt/L +/-1 72 0.0593 pCi/L +/-0 168 N/A NXP2 11/11/13 09 58 95 5 (75%-125%) 11/06/13 09 58 1/11/13 09 58 Uncertainty 174 Uncertainty Uncertainty 62 2 53 9 pCi/g 14 2 +/-1 72 +/-1 71 16 7 pCi/g +/-0.929 U 0 372 pCi/g +/-0 171 (0%-20%) JXH2 11/11/13 10.10 96 2 (75%-125%) 1/11/13 1010 11/1113 10 10 Uncertainty 20 5 Uncertainty Uncertainty 24 7 +/-1 29 23 0 +/-1 22 22 1 +/-1 15 -0 0144 +/-0 0632 pCi/g 7 22 pCi/g pCi/g (0%-20%) JXH2 11/08/13 10 44 108 (75%-125%) 1/08/13 10:44 11/08/13 10 44 859 898 pCi/g 4 49 (0%-20%) HAKB 11/08/13 12-01 Page 79 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Workorder: 336330 QC Summary Page 2 of 4 Parmname NOM Sample Qua! QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1342000 QC 1202975004 LCS Thonum-230 QC 1202975002 MB Thonum-230 Batch 1342001 QCI202975006 336330022 DUP Uranium-238 QC 1202975007 LCS Uranium-238 QC 1202975005 MB Uranium-238 Rad Gas Flow Batch 1342067 QC1202975222 336330004 DUP Lead-210 QC 1202975223 LCS Lead-210 QC 1202975221 MB Lead-210 Batch 1342068 QC1202981563 336330019 DUP Lead-210 QC 1202981564 LCS Lead-210 QC 1202981562 MB Lead-210 Batch 1342069 QC 1202975225 336330032 DUP Lead-210 QC1202975226 LCS Lead-210 QC 1202975224 MB Uncertainty 20 4 Uncertainty Uncertainty Uncertainty 25 5 Uncertainty Uncertainty Uncertainty 204 Uncertainty Uncertainty Uncertainty 207 Uncertainty Uncertainty +/-6 54 +7-7 82 189 +/-1 22 0 325 +/-0 245 pCi/g pCi/g 929 (75%-125%) HAKB 11/08/13 12 01 1/08/13 12 01 185 +-/-4 54 209 +/-4.95 27 2 +/-1 44 0 00 +/-0 0717 pCi/g 12 4 pCi/g pCi/g (0%-20%) HAKB 11/09/13 1135 107 (75%-125%) 11/09/13 11 35 11/09/13 11 35 362 +/-3 90 393 +/-4.37 190 +7-2 81 -0 0292 +/-0.360 pCi/g pCi/g pCi/g 8 40 (0%-20%) KDFl 11/13/13 08 48 93 5 (75%-125%) 1/13/13 08 33 11/13/13 08 48 238 +7-3.34 215 +7-3 01 195 +7-2 66 1 10 +7-0 324 pCi/g 10 2 pCVg (0%-20%) KDFl 11/13/13 09 45 94 3 (75%-125%) pCi/g 11/13/13 09 45 11/13/13 09 45 U 3.09 U 2 42 pCi/L N/A Uncertainty +/-1 29 +7-1 45 N/A KDFl 11/13/13 11:23 22200 Uncertainty 18500 pCi/L +7-56 3 83 5 (75%-125%) 11/12/13 14 24 Page 80 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www gel.com Workorder: 336330 QC Summary Page 3 of 4 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gas Flow Batch 1342069 Lead-210 Rad Ra-226 Batch 1342217 QC 1202975633 336330032 DUP Radium-226 QC 1202975635 LCS Radium-226 QC 1202975632 MB Radium-226 QCI202975634 336330032 MS Radium-226 Batch 1342297 QCI20297580I 336330001 DUP Radium-226 QCI202975803 LCS Radium-226 QC1202975800 MB Radium-226 QC1202975802 336330001 MS Radium-226 Batch 1342298 QC1202975806 336330016 DUP Radium-226 QC1202975808 LCS Radium-226 QC1202975805 MB Radium-226 QC1202975807 336330016 MS Radium-226 Uncertainty 1 78 pCi/L +/-1 22 11/12/13 14 23 U 0.268 U Uncertainty +/-0.117 24 7 Uncertainty 0.521 pCi/L +/-0.137 21 9 pCi/L +/-0 680 N/A N/A KSD1 11/06/13 12.35 ;7 (75%-125%) Uncertainty 24 7 U -0 0532 +/-0.0996 pCi/L 0 268 Uncertainly +/-0 1 17 23 6 pCi/L +/-0 739 95 8 (75%-125%) 11/06/13 13 05 11/06/13 12 35 11/06/13 12 35 Uncertainty 18 5 Uncertainty Uncertainty 18 5 Uncertainty 149 +/-1 73 161 +/-I 87 pCi/g 7 99 (0%-20%) KSD1 11/12/13 14 45 15 9 pCi/g +/-0 520 85.5 (75%-125%) 149 +/-1.73 0 251 +/-0 110 203 +/-1.96 pCi/g pCi/g N/A (75%-125%) 11/12/13 14 45 11/12/13 1410 1/12/13 14.45 Uncertainty 17 7 Uncertainty Uncertainty 193 Uncertainty 146 +/-1.95 121 +/-1 85 pCi/g 18 9 (0%-20%) K.SD1 11/09/13 18.05 20 0 pCi'g +/-0 715 113 (75%-125%) 0412 +/-0 153 pCt/g 146 t-'-l 95 150 pCi/g +/-1 87 N/A (75%-125%) 11/09/13 18 40 11/09/13 18-05 1/09/13 18 05 Notes: Counting Uncertainly is calculated at the 68% confidence level (1-sigma) The Qualifiers in this report are defined as follows. ** Analyte is a surrogate compound Page 81 of 82 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Workorder: 336330 QC Summary Page 4 of 4 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time < Result is less than value reported > Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample F Estimated Value H Analytical holding time was exceeded K Analyte present Reported value may be biased high Actual value is expected to be lower L Analyte present Reported value may be biased low Actual value is expected to be higher M M if above MDC and less than LLD M Matrix Related Failure N/A RPD or %Recovery limits do not apply Nl See case narrative ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier 0 One or more quality control criteria have not been met Refer to the applicable narrative or DER R Sample results are rejected U Analyte was analyzed for, but not detected above the CRDL UI Gamma Spectroscopy—Uncertain identification UJ Gamma Spectroscopy—Uncertain identification UL Not considered detected The associated number is the reported concentration, which may be inaccurate due to a low bias X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL Concentrations are <5X the RL Qualifier Not Applicable for Radiochemistry. h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone by a factor of 4 or more " The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL) In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result * Indicates that a Quality Control parameter was not within specifications For PS, PSD, and SD1LT results, the values listed are the measured amounts, not final concentrations Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 82 of 82