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HomeMy WebLinkAboutDRC-2006-001144 - 0901a0688080569dFOURTH QUARTER SEMI.A}[NUAL RADIONUCLIDE EMISSIONS TEST CONDUCTED AT TNTERNATTONAL URANTUM (USA) CORPORATTON NORTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE BLANDING, UTAH October 17-18,2006 by: TETCO 90 East Main Lehi, UT 84043 Phone (801) 768-0973 Fax (801) 768-0880 Prepared for: International Uranium (USA) Corporation 64255 Hwy 91 Blanding, Utah 84511 Date of Report: October 25,2006 CERTIFICATION OF REPORT INTEGRITY Technical Emissions Testing Company (TETCO) certifies that this report represents the truth as well as can be derived by ttre methods employed. Every effort was made to obtain accurate and representative data and to comply with procedures set forth in the Federal Register' Dean A. Kitchen Reiewer: ,&za-rz'VfuDut", //-w- TABLE OF CONTENTS PAGE Introduction TestPurpose ........ Test Location and TYPe of Process TestDates....I I Pollutants Tested and Methods Applied Test ParticiPants Deviations From EPA Methods Quality Assurance Summary of Results Emission Results Process Data . Description of Collected Samples . ' Discussion of Errors or lregularities Percent Isokinetics Source Operation Process Control Devices Operation Process RePresentatlveness Sampling and AnalYsis Procedures SamplingPort Location . . . . Sampling Point Location Sampling Train DescriPtion . . . Sampling and Analytical Procedures Quahty Assurance Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related CorresPondence 6 6 7 7 LIST OF TABLES Measured Radionuclide Emissions ' ' ' Percent Isokinetics SamplingPointlocation'' ::''' PAGE Table I II m IV V J 4 6 C""-ripf"t" Results, North Yellow Cake Scrubber Complete Results, Yellow Cake Dryer Baghouse Appendix A Appendix A Figure I 2 aJ LIST OF FIGURES Schematic of Method 5lll4 Sampling Train Facility Schematic Representation Io* Yellow Cake Scrubber F;.iitty Schematic Representation-Yellow.Cake Dryer Baghouse Appendix D Appendix D Appendix E INTRODUCTION Test Purpose This testwas conducted to determinethe total radionuclide emissions fromtheNorth Yellow Cake Scrubber and Yellow Cake Dryer Baghouse exhausts in terms of Curies per dry standard cubic foot (Cildscf). Test Location and Type of Process International Uranium (USA) Corporation is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Dryer Baghouse. The Packaging enclosure also discharges into the Dryer Baghouse. The North Yellow Cake dryer was the only operating dryer at the time of the test. The South Yellow Cake Dryer is currently not operational. Facility schematics are shown as Figures I and2 in Appendix D. Test Dates Two test runs on the North Yellow Cake Scrubber and the first test run on the Yellow Cake Dryer Baghouse were completed on October 17,2006. A second test run on the baghouse was completed the following day on October 18fr. Pollutants Tested and Methods Applied The tests were a determination of radionuclide emissions in accordance with EPA Method 5/rt4. Test run filters and front wash residues were sent to Energy Laboratories in Casper Wyoming for radionuclide analysis. Test Participants Test Facility State Agency TETCO Wally Brice None Paul R. Kitchen David Turk Joseph Kitchen Mike Ransom Deviations From EPA Methods None Ouality Assurance Testing procedures and sample recovery techniques were according to those outlined in the Federal Register and the Quality Assurance Handbookfor Air Pollution Measurement Systems. SUMMARY OF RESULTS Emission Results Table I presents the findings ofthe test in Curies per dry standard cubic foot. Tables [VandV in Appendix A have more detailed information. Yellow Cake Dryer Baghouse AVE I 2 7.1728+03 Process Data The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow , pressure, and baghouse pressure drop readings (Ap) were recorded and are found in Appendix D. Production data will be submitted by International Uranium. Description of Collected Samples The filter on the frst test run on the North Yellow Cake Scrubber was covered with a white colored particulate. The second filter on the scrubber was covered with a yellowish colored particulate. The front washes were clear in appearance. The filters for both test runs on the Yellow Cake Dryer Baghouse had no visible particulate on them. The front washes were clear in appearance. Discussion of Errors or Irregularities 9.459E+03 4.884E+03 North Yellow Cake Scrubber 23.49r 3s.007 2.2238+06 2.949E+06 None Percent Isokinetic Sampling Each ofthe tests were isokinetic within the Ll}yoof 100% criterion specified in the Federal Register. They also meet the Utah state Deparfinent of Environmental Quality' Division of Air euahfy specification of isokinetic sampling ioint by point. Isokinetic values for each test run are presented in Table II- Yellow Cake Dryer SOURCE OPERATION Allprocesscontroldeviceswereoperatednormally'Recordedscrubberwaterflow'pressure and baghouse Ap readings were recorded and are found in Appendix D' Process Representativeness The facility was operated normaily. production data will be submitted by rntemational Uranium. l I Sampling Port Location The inside diameter of the North Yellow cake Scrubber stack is l8'0 inches' The two' four- inch diameter sample port are located 6.3 diameters (9.5 feet) downstream from the last disturbance and 6.3 diameters (9.5 feet) upstream from the next disturbance' Figure 1 in Appendix D is a schematic of the stack. The inside diameter of the Yellow cake Dryer Baghouse stack is 16'0 inches' The two' four- inch diameter sample ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 diameters (57 inches) upstrearrr from the next disturbance. The sample port locations are depicted in Figure 2 in Appendix D' Sampling Point Location Table III shows the distance of each sampling point from the inside wall according to EPA Method l. Each point is marked and identified with a wrapping of glass tape and numbered' These ;;il are determined by measuring the distance from the inside wall' Distance (inches) from Inside Wall 0.s8 1.89 3.49 5.81 t2.19 14.51 16.11 APPENDIX A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related CorresPondence APPENDIX A Complete Results North Yellow Cake Scrubber Yellow Cake Dryer Baghouse Nomenclature Sample Equations A Norh Yellowcake TABLE IV COMPLETERESULTS, PM INTERNATTONAL URANILIM CORPORATION (ruC) NORTH YELLOWCAKE SCRUBBER EXHAUST Symbol Date Filter # Begin End Description Dimensions Run #l t0/17/2006 4848 8:27 ll:47 24.15 1.551 1.004 r57.917 89.5 0.3368 561.0 r92 0.84 0.3715 1.80 17.80 80.40 t23.547 26.451 0.1060 0.894 29.00 27.83 95.8 . 109.3 1.767 -0.03 24.08 24.078 1.588+03 2.368+03 1.34E+03 2902.2 23.4907 2.223fi+06 Run #2 r0/17/06 4849 l2:14 l5:30 24.15 1.494 1.004 160.779 97.3 0.3086 685. I r92 0.84 0.3805 2.20 18.20 79.60 124.004 32302 0.1290 0.871 29.08 27.65 r02.9 1r6.2 r.767 -0.03 24.08 24.078 1.40E+03 2.19E+03 1.24E+n3 4341.0 35.0070 2-9498+A6 Date Time Test Began Time Test Ended Pb. Meter Baromefic Pressure AH orifce Pressure Drop Y Mctgcatrbration Y Factor Vm Vohmc Gas Sampled-Met€f, Conditions T- AvgMelcrTcmp€rahre JAP Sq Root velocity Head Wt-" Weight Watcr Colteaed T, Duration of Test Ce Pitot Tube Coefficient Do Nozzte Danreter COz Vohme % Carton Dioxide 02 Volume%Oxygen N2 & CO Volme o/o Nitrogen and Carbon Monoxide Vn\a Volume Gas Samplcd (Stanrlrd) Vw Volume watcr vapor Bw. Fraction HrO in Stack Gas Xd Fraction of Dry Gas Md Mol€culatwt. Drycas M. Molcculd Wt. Stack Gas %l P€rcent Isokinetic T" AvgStackTemperature A* $ack Cross Sectional Area PC StackstaticPressure Pbo Sample Port Barometsic Pressure P" Stack Prcssre Q" Stack Gc Volureric Flow Rate (Std) Q" Stack Gas Vohmetic Flow Rate (Actual) V" Velocity of Stack Gas Curies Radionuclidcs per sample Cfad ConceotrationofRadionuclides ERrad Emission Rate of Radionuclides In. Hg. Abs In. I{rO dimensionless cf I Root In. H2O Grams Minutes Dimmsionless Inches P€rcflt Percent Percent dscf scf Fraction Fraction lMbrml lMbmol Perc€nt "F Sq. Ft. In. HrO In. Hg Abs In. Hg. Ab6 dscfu cfin fpm pci pCildscf pCi/ht AVG 112.8 1.49E+03 2.278+03 1.298+03 29.2488 2.5868+06 Saturated moisture fraction used in all calculations for runs l& 2 as the mea.liur€d moisture was supersaturated BagtroGs€ TABLEV COMPLETE RESULTS, PM TNTERNATIONAL URANruM CORPORATION (ruC) YELLOW CAKE DRYER BAGHOUSE DimensionsSymbol Date Filter # Begin End Pb. AH Y Vm T_ r/lp Wt*c T, ce Dn Coz o2 N2&CO vmoa Vw Bw, xd Md M, %T Description Run #l t0/1712006 4809 l6:38 19:46 24.t5 1.983 1.004 172.791 92.1 0.3462 25.7 180 0.84 0.37t5 0.00 20.90 79.t0 134;723 1.2r2 0.009 0.991 28.84 28.74 98.0 94.1 r.396 -0.11 24.08 24.072 1.42E+03 1.86E+03 1.33E+03 15.0 0.11l3 9.4598+03 Run#2 l0/l 8/06 4810 7:40 l0:41 24.45 1.905 1.004 168.757 86.3 0.3390 22.6 180 0.84 0.3715 0.00 20.90 79.10 134.585 1.066 0.008 0.992 28.84 28.75 98.7 87.8 1.396 -0.1I 24.38 24.372 l 40E+03 1.80E+03 1.298+03 7.8 0.0580 4.884E+03 T. ,\ Pc Pbo P. Q" Q" v" Curies Crad ERrad Date Time Test B€g:an Time Test Ended Metcr Barometric hessure Orifice Prcssne Drop Meter Calibration Y Factor Volune Gas Sampled-Meter Conditions Avg Meter Temperaire Sq Root Velocity Head Weight Wat€r Collected Duration ofTest Pitot Tube Cocfficient Nozde DiarEter Volume % Carton Dioxide Volune 7o Orygen Volune 7o Nitsogelr and Cabon Monoxide Volme Gas Samplcd (Standard) Volume Water Vapor Fraction H2O in Stack Gas Fractior of Dry Gas Molecular Wt. Dry Gas Molecular Wt. Stack Gas Percent Isokinetic Avg Stack Temperanre Stack Cross Sectional Arca Stack Static Pres$re Sample Port Barometic Pressure Stack hesstne Stack Gas Volumeric Flow Rate (Std) Stack Gc Volllrctic Row Rate (Actual) Velmity of Stack Gas Radionuclides per sample Concentratiol of Radionuclides Emission Rate of Radionuclides ln. Hg. Abs h-H2O dimensionless cf T Root In. H2O Grams Minutes Dimeosionless Inches Percent Perc€nt Perccnt dscf scf Fraction Fraction lb/lbmol lb/lbnol Percent F Sq. Ft In- HrO In. Hg. Abs In. Hg Abs dscfin cfin $m pci pCi/dscf pCi/hr AVG 91.0 l.4lE+03 l.83Er{3 1.318+03 0.0E46 7.1728+03 M5 Nomenclature Yol: percent isokinetic, percent As: stack cross-sectional area (ft3) ASAP: ree {AP Btu : unit heat value (British thermal unit) B*r: fraction of water in stack gas Cs : concentration of particulate matter, back half (grldscf,lb/dscf, etc.) Cs: corc€ntration of particulate matter, front half (grldscf,lb/dscf, etc.) C."t"l: concentration of metals (pp-, trdft', etc') atomic symbol replaces "metal" COz: percent carbon dioxide in the stack gas Co: pitot tube coefficient (0.84) - Cx 1uog1: species symbol replaces x ' Cx (.o,,): actual gas concentration corrected to required percent 02 AH: orifice pressure drop (inches H2O) AHq : orifice Pressure (inches H2O) AP : 51ask flow pressure differential (inches H2O) Dr: diameter of the stack (feet) Do: nozzle diarneter (inches) EA: percent excess air ERg : emission rate of back half particulate (lblhr) ERr: emission rate of front half particulate (lbAr) E&n-s* : emission rate per mmBtu or ton of fuel etc. ERx : emission rate of compound which replaces x k-fact = multiplier of test point AP to determine test point AH L = length of rectangular stack (inches) mBtu: thousand Btu M4: flolecular weight of stack gas, dry basis (lb/lb-mol) Mp: rnoSS of particulate on filter (mg) Mrp: mass of particulate matter on filter and probe (mg) mmBtu: million Btu Mp: lnaSS of particulate matter in probe (mg) Mr: molecular weight of stack gas, wet basis (g/gmol) N2 : percent nitrogen in the stack gas 02 : percent oxygen in the stack gas {AP = average of the square roots of AP (may also be referred to as ASAP) Pb-: absolute barometric pressure at the dry gas meter (inihes Hg) Pbo: absolute barometric pressure at the sample location (inches Hg) P6 = stack static pressure (inches H2O) P, : absolute stack pressure (inches Hg) P,6: absolute pressure at standard conditions (29.92 inches Hg.) e - time of test (minutes) Q": stack gas volumetric flow rate (acfm) Q.: stack gas volumetric flow rate (dscfm) Qw: wet stack gas std. volumetric flow 1ft3/min, wscfin) Ts : stack temPerafure (oF) Tr,6: absolute ternperature at standard conditions (528T') Tt: see 0 I I M5 Nomeirclature U un = mean molecular speed (cm/s) ,. Vm = samPle volume (ft1 at meter conditions ,l 'l_ Vm",6 = volume standard (dscf), sample volume adjusted to 68T and29-92 inches Hg. Vr: velocityof stack gas (fpm) I ; Vwc= volumewatervapor(scf)at68Tanda9.9?inchesHg.L W = Width of rectangular stack (inches) , Wqrc = weight ofthe condensed water collected (grams) It- Xo = fraction of dry gas Y = meter calibration Y-factor (dimensionless) I i1 i IL I1jL L- L L I Method 5 - 7oI = Vmo6. (T, + 460)' ll3g /(0'Vr'Pr'Xa'Dn2) A,=(Ds2 /47'n Bo,. = V* / (Vmrn6 +V*) Cs: Me ' 0'01543 / Vm'6 Cr: MrP'0'01543 / Vm'6 Cx ("o,)= Cx(uue) . (2O.9 - desired %O2) I (209 - actualYoO2) D*:2.L.W/(L+W) Dnd", = {{o.ozoq . (Pb, + 0.0735) / [(T, + 460)' Cp' Xd' {(t, + 460)' M,) / (P,' AP)]} EA: (o/oO2-0.5%CO) /10.264 7Nz - (%Oz- 0'5 %CO)l ERs = Cs'Q" 0'00857d ERr: Cr' Q.' 0'00857 E&".s* = ERx / (mmBtu / hr) K-fact=846.72.Dn4.AH6.Ci.XiiMa'P,'(T.+460)/[Mr'(Ts+460)'(Pb'+AH/13'6)] M6: CO2 . 0.44 + Oz. 0.32 + N2 '0.28 Mr: (Ma ' XJ + (18 'B,'s) Pr: Pbo + GG / 13.6) Qo = V. 'A, e Q, = Qa. Xd. Ps. T.16 / [(Ts + 460)'P$d] Qw: Q, / Xa Vmoa : Vm . Y' Trtd' (Pb. + AH i 13 -6) / [Poa' (T. + 460)] v, = 85.49 . 60 . Cp . {AP '{ Kr, + 460) / (P, 'M,)l V*": Wt*"' 0,04715 X6: I - B"u PreliminaryN Y Cake Scrb Facility lnternatlq44! Uranium APPENDIX B North Yellow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data Yellow Cake Dryer Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data Sfttf ri"tdDatasheet Plant: lnternational Uranium Assumed Moisture 4-16% Probe 2? C. Nozzle Calibration cp 0.84 ,3'r , Jl_L .37t ,31_? AvgDn .i7 lLins11e5 cas eag@[ Console 5 v-Yaaorlafi- ^H@!:Z_lt_int2o Barometric Pressures va^ 29' /5 inug pu, 2?.O ff inttc -.o3 Lcak Checkr Pre Post a'ninp.1/l! a.Cf 't vacinHg-/./- / Z PitotRatc ?' d O.n.2-3lnHrO 'Z5 Fl IWaterCollected J6l g Total rq4 t-l J lMpza,rz_gET, Time Sampled /CZ min Review -TF- K=/'.2 I lrrrco t I Fnrcr-fu!fi- Sample Box-[- Lo"ution, North Yellow Cake D Operator: t1q4 f/7 6v> Pase / of/ Run# I t I /\ I\,1V I A Diameter 18" Port Reference :Ul- are gupstream from next disturbance are 9.5' Downstream 1 5 Commcnts:,t9lt7 a t3.7 | K= l3'Ll6 td dr0 @T'n @T^A lll 5f .,r t1 rirrd Dara sheet ptanr lnternational Uranium Datc O +.6c:r 1-r, Za4l . /cf.774,/ tffie&?r- I L",ro I I Fitter -kj! 1' - ii'ion t*0- Location: North Yellow Cake Dryer Scrubber -- owtor: /Y7 t la.- R ^ n lott /\-1 I\/\_/ I tt Stack Diameter -![_ Port Reference 0" are __94_Upstream from next disturbance arp 9.5' Downstream from last disturbance I Run # Time Samplcd | 7 Z- min Review I fz-. ''I nL II Pogr-..,1 orj Assumed Moisture 4-16 % Probc 3{ 6- "o - o.aa Nozzle Calibration^;ffi-"Ja -TrJ 3 tro l*sfiV,3f05n n, crsYagt'j3 Console 5 Y-Factor / , Ooq LHg,z.frF inH2O Barometric Pressures Yb^ 7q,/9 tnr, wo ??.df, inwg pn -,d7 in:Hro kak Chcck; &9 Post rf,.in d,O()Carvrcin}lg L I Pir<l.at. O, O InHrO , ? S+ watercollected L8S'l Total 4 Iit$/ L1'1'/ s- |O $tt l. qq{ ' Tnvw Point t(5q 3l tL\ "/ ^,.,* ,.4+rtt.#'t'r* tt6.z ' "o2"/ i:l:'] T;i;i ts.c 100 N Stac* Dia- Ports are Ports are 16"Reference: Ott 57"Upstrcam from next disturbance Downstream from last disturbance Preliminary Y Cake BH Comments: Facility lnternational Uranium Stack Identification Yellow Cake Dryer Baghouse Date to I tTJo Barometric Pressure Pb- Jel.l5 inHg Pbo 24.o8 inHg Static hessure (Pc) -, l, in HzO Estimated Moisture (Bw)IN Sample Height from Ground 70 feet Averages: Tr_ zFlow aP {aP Ts lFlow AP Traverse Point Percent Diameter Distance From:Ports ID Reference A B c D E F I 4.4 0.70 0.70 .{rt.oq5' 2 14.6 2.3.4 2.34 j I aJ 29.6 4.74 4.74 .I 15. t,<.i 4 70.4 lt.26 tr.26 k 5 85.4 13.66 13.66 7 4, .tn\o' 6 95.6 15.30 15.30 L 'l KEY:> t( Field Data Sheet l,erco I t 4ritter-tlXQl SampleBox Location: Yeflow Cake Dryer Baghouse operator: Jog K;lchcn Pagelo( Run# | Plant: Date: International Uranium lo - l-t -ok Assumed Moisture 1o/o Probe / t- q cp 0.84 Nozzle Calibration.bu .5?L .37( .Az- AugDn.fl5inches Gas Bag ambient Console 5 t-t'6st61 l.AO'&l AHq_UtlLin Hzo Barometric Pressures Pb' zcl' It in Hg Pbo ?-4'ox in:Hs P" --l\ inHzo Lcak Check; Pre Post nlmin .Oo,. .WL uu",nHg 2D 5 PitorRarc o'ff-) (2'oo hH2Q 3 ,1- Water Collected Time Samplcd Review mtn t?1. 111 "/_el_J519 t 7\.<( ,,. lll-jr r./L?- l0 tr' Tnwnc Point toL /\o1 ) \/l')P Diameter 16" Port Reference 0" Ports are 57" UDstream from next disturbance are 468' Downstream from lastdisturbance ! Commcntg: r ,9,1v2- r 1 .1X3 ,z ricta pL srr"et I Plant: Intemational Uranlum Datc: lD - lQ - nr- I I .jrcd Jrirter{@ SampteBox_fi_ Location: Yellow Cake Dryer Baghouse opcrator: Jre K$<_Acl t Run# Z Assumcd Moisture 1o/o ttProbe I + -q cp 0.84 Nozzle Calibration.37t .372 .3?t .37L lven" . j75 inches Cas Bag ambient Console 5 Y-fu",or.lJf, AH@ l.5tE in Hzo Barometric Prossures pu, Z{.tt f inne Pb, 2-Ll-3a in:Hs pa -.\\ inH2o Lcsk Chect: Pre PgS!ftlmin.Oos , OOt vrcinHe Z0 5 PitorR*c O.oO O.OO htzo .L , ?L Water Collccted 2? . (? g Time Sampted /,f,D min Rcview JU- ttl Page-Lof_| Trres Point o ll4&"flL1 'et$?t 2t.* /t?A / V1.x z ]dlo z A^t I/)F Diameter 16' port Reference 0, Ports are 57' Upstream fiom next distwbance Ports are 468" Downstream from last disturbance L:371o,t.1 lt.t ,K= K= @T, @Tr pt',t Tn\er***trtJ Vranv'* Analytical Method---JfRiS,t!!- ox" pfft/ob Test No. I GasBagNo. lV-O3 )ttnbient TemP 7Q Operator -l?Flt:- TestNo. Gas Bag No. -mbient TemP OPerator Test No.- Gas Bag No. \mbient TemP - OPerator RUN Averege Net Volume Gas 2 Actuel Rcrding Ncl Actuil Reeding Ncl Actual Reading Nct Coz l,g ,.9 I.?t.?,.8 l-g t.e Dr (Net is Actual 02 Reading Minus Actual -f)- Readinp) t1.b fi.6 t?-(s t?.8 , ?.6 17.8 17,9 N2 (Net is 100 Minus Actual Ot Reading).8o.l fu-Ll ,o .1 80.v Date to/lr/ae 7 F -osTlPP RAN Average Net Volune Gas I L J Actuel Reeding Nct Actud Rcrdirg Nct Actuel Rceding Nrl Coz 2.7 L.L z.z z.L z.?z-z z.z t8 .L zo./tg -z )(t.zO, (Net is Actual 02 Reading Minus Actual CO^ Readins).7o..1 t9.Z 7o.7 N2 (Net is 100 Minus Actual 02 Reading).7?.t'ft.o 7?.a n6 RUN,il.tll3tll Averagc Net Yolume Gos Actud Rcrding Net Acturl Rceding Ncl Acturl Rerding Nct Coz 02 (Net is Actual 02 Reading Minus Actual lO^Readins)- N2 (Net is 100 Minus Actual Or Reading). CO is not measwcd, as it has thc same molecular weight as N2 Llg0 1 7o/n/oo Initials PPt' I I Final (gl lnitial e1 Net 1g1 Final (e) Initial lgl Net 1g1 I I Total(s)22.(t ml 'Initials Final (gl Initial ts) Net 1s; itial I Net .. s Net , ' c+ l'32 g/ml= Volume of liquid (H1O) in .FilterNumber: iiirirrrcTn.$ Filter Number: : Final ' . g fze Sample Bo.xi Chain of Custody and Analytical Request Record PLEASE pRINT; provide as much information as possible. Refer to corresponding notes on reverse side. I Page 1 of 1 Gontact Name: Wally BriceVoice: 435-678-2221Fax: 435-678-2224 Email: Furchase Order #:lnvoice Contact & Phone #: Same Notify ELI prior to RUSH sample submittal for additional charges and tE Io FIoftr ia*\*eLY" t& t4*Id.#11,} ffi&'f'#il} E*,'Eao€; E.=co E 3 iBigq€a"EEi SrS-o.=o<t>l MATRIX Comments: Contant Wally Brice for required analysis. Each samPle consists of a glass fiber filter and beaker residue Combine filter and beaker results Sampfe volume 123.547 dsd Combine filter and beaker results10t17106 Sample volume 124.004 dscf Combine filter and beaker results Sample volume 134.723 dscf Combine filter and beaker results Sample volume 134.585 dscf Relinquished by: Date/Time: Company Name: International Uranium Report MailAddress: 6425 South Hwy 91 Blanding, UT 84511 lnvoice Address: Same Report Required For:POTWAAAA/TP Other - Special Report FormFELl must be notified prior to sample submiftal for the following: NELAC n A2LA ! LevellV f] Other _ EDD/EDT fI Format SAMPLE IDENTIFICATION (Name, Location, Interval, etc) ' 4848 Filter 2 q848 Beaker t 4B+9 Fitter o 48+9 Beakert +809 Fitter " 4809 Beaker ' 4810 Filteru +810 Beaker Custody Record MUST be Signed Project Name, PWS#, Permit #, Etc. Sampler Name if other than Contact: PaulRKitchen/TETCO 801-768-0973 ELI Quote #: Receipt Temp _oc Cooler lD(s) Custody SealY N lntact YN Signature Y N Match LAB ID Received by: Dateffime: Dateffime: LABORATORY ONLY # of fractions h c!d'h cirmr.lc.s, smprer luhnhEd ro EFry Llbor.tdic!, r,* rv t. *t*"tu[ffillf;;iot* * '-"i! Fqu6r'( 'IhB s"v's s nori@ of rhk D6!itiritv arr 3ub'conrrt 'ld! Page I ofl - Dean Kitchen From: Kerri Schroeder [kschroeder@energylab'com] - Sent MondaY, November 27'20CF.1:08 PM To: tetco-ut@qwest'net - Subiect: Filters combined with beakers -Kprri Scfiroefer Technical RePorter EnergY Laboratories, Inc' -2393-Salt Creek HwY (82601) PO Box 3258 CasPer WY 82601 -l-888-235-0515 (307)-23s-0sls "-*"it kschroeder@energylab'com -Visit our Web rag;at Utti:tiwurw'energytab'corr/ This transmission is GONFIDENTIAL. If you have received this in error, please contact ENERGY LABORATORIES' -INC. immediatelY. ENERGY IABORATORIES,"VC' ' 2393 SaltCrcek Highway (82601)* POBox3258 ' CasPer,Vhf 82602 Client: Proiect: Lab lD: ClientSamPle lD: LABORATORY ANALYTIGAL REPORT lntemational Uranium (USA) GorP Not lndicated c06101356-001 4848 Filter Combined Wih 4848 Beaker RePort Date: 11127106 Collection Date: 10/17106 DateReceived: 10/30/06 Matrlx: Filter Result Unlts Quallfier RL ilcu OCL Method Analysb Date, BY Analyses MDIONUCLIDES .TOTAL Lead 210 Radium 226 Thorium 230 Thorium 230 Precision (t) Uranium, Activi$ ND Pci/FilterND PCi/Filter 1.5 PCi/Filter O.7 PCi/Filter 2900 PCi/Filter 1.0 0.2 0.2 0.2 NERHL65-4 E903.0 E907.0 E907.0 sw602o 11/06/06 12tr,0 t il 11/10/06 16:47 I ctt 1'tt15lc6 15:00 / df 1 1/15/06 1500 / df 1110UCF 21:15 /hrs Report Delinltions: RL - AnaMe rePorthg limil QCL - QualitY control limit. MCL - Ma<imum contaninant let'd' ND - Nct detected at the reporiing limit' ENERGY LABORAIOR ES, [VC. * 2393 SaftCteek Highway (82601) 82602 ' POBox328 * @sPer,W LABORATORY ANALYTICAL REPORT lntemational Uranium (USA) CorP Not lndicated c0610135G002 Client Sample lD: 4849 Filter Combined With 4849 Beaker Client: Project: Lab lD: RePort Date: 11127106 Collection Date: 10/17106 DateReceived: 10/30/06 Matrix: Filter Result Units Qualifier MCU QCL ]ttethod Analysls Date I BY Analyseg RADIONUCLIDES .TOTAL Lead 210 Radium 226 Thorium 230 Thorium 230 Precision (t) Uranium, Activity ND pci/Filter ND pCi/Filta 0.6 pCi/Filter 0.4 pCi/Filter 4340 pCi/Filter 1.0 0.2 0.2 0.2 NERHL65'4 E903.0 E907.0 E907.0 sw6020 1 1/06/06 12100 I Pl 11/10/06 16:47 I ott 1 1/15/06 15:00 / df 11/15/06 15$0/df 111021c6. 21 :33 / bMrs Report Ileflnltiotts: RL - AnaMe rePorting limit. QCL - Quality conrol limit. MCL - Maxirnum contaminant level- ND - Notddected dthe reporting limit' ENERGY LABORATORIES, INC' ' 2ggg SaltCrcek Highway (82601)' PO Box 3258' CasPer, llWffi Client: Project: Lab lD: Client SamPle lD: 82602 LABORATORY ANALYTICAL REPORT lntemational Uranium (USA) CorP Not Indicated c0610135G003 4809 Filter Combined Witt 4809 Beaker RePort Dabl: 11127106 Goltection Date: 10/17106 DateReceived: 10/30/06 Matrir Filter Analysb Date, BYMCU Qualifier RL @L MethodResult Units Analyses RADIONUCLIDES .TOTAL Lead 2'10 Radium 226 Thorium 230 Uranium, Actfuity 1.0 0.2 0.2 0.2 ND ND ND 15.0 pCi/Fitter pGilFilter pCi/Filter pCiiFitter NERHLSil 11/06/06 12flO lPt E903.0 11110/ffi 16:47 toil E907.0 11/t5/06 15$o/df SW6020 |lrcAcxd 21:36 / buts Report Ileflnitlons: RL - Andyte rePorting limit' OCL - Ouality cmtrol limit' MCL - Maximum contarninant level' ND - Not detected at the reporting limit' I i- M ENERGY LABORATORIES, ttlC' ' 2393 SaftCrcek Highway (82601), POBox325E' @sPr,WY 82602 Client: Prciect: Lab lD: GlientSamPle lD: LABORATORY ANALYTICAL REPORT lntemational Uranium (USA) CorP Not lndicated c0610135ffi04 4810 Filter Combined Wih 4810 Beaker RePort Date: 1127106 Cotlection Date: 10/18/06 DateReceived: 10/30/06 Matrix: Filter Result t nlts Qualifier MCU QCL Method Analysls Date I BY Analyses RADONUCLIDES'TOTAL Lead 210 Radium 226 Thorium 230 Uranium, Activi$ ND pCi/Filter ND pCi/Filter ND pci/Filter 7.8 pCi/Filter 1.0 0.2 0.2 0.2 NERHL6-$4 11/06/06 '12:Oo | 7i1 E903.0 11110106 20:44 I ott E907.0 11/15/06 15$0/df SW6020 11102/c6 21 :'10 / b\"s Report D,eflnitlotts: RL - Anatyte reporting limlt. QCL - Quality contrd limit. MCL - Maximum contaminant le\d' ND - No[ d€fected at the,eporting limit' APPENDIX D North Yellow Cake Scrubber Figure 1. Facility Schematic Representation Scrubber Process Data Yellow Cake Dryer Baghouse Figure 2. Facility Schematic Representation Baghouse Process Data D Inte rtnati onal UraniumFacility: stack rdentincation: North Yellow Cake Scrubber t C[ I#t I I I I a: Distance upsteam from next disturbance, feet p: Distance downsteam from last distwbance, feet y: Distance of Sample Level to floor, feet Q: Stacklnside Dianeter, inches Estimated Moisture, percent Estirnated Temperature, T Estimated Velocity, fPm Number of Ports 9.s', 9.5' 18" Near Saturation 70-t25 1.100 l+o+l Control Unit Type: Figrre 1. Facility Schematic Representation f ;27 | 1/'\<- !; to X:03 1;L8 70io/ f0 "euI,a'5z ll', t7 llt so tttn\q S."doJrr w"/". {/a^, 6P>- g .'/g3 I .,/ g,Lf 8,.1 €.4 8,y 84 fu* S..of,f,t, 12:)Z tL 5T 13 tz3 f3"L/O I1'r49- t5',9 5 _/g; z_7 a.y 8,f I .rl 8rfg,{ 8,r <,{I ,11, I vof; fl* 6fn 1,8 ,1,7 4,8,{-? Ll 4 q.8 /"84,8 1.8tl ,V 4,9tl 'g 1,1,4;?_ ,,q,a' tl t7-.; 5rnj Ln Prearrz<_ 1t. I 1,1q"( q.( q, Z-.--q,l {,L44 q"t ,{ .t '{, /,({,/ ':4"{,; '4 '"2''i zl , Z'- Faci,i,y: International L]ranium l+a+l t (l .l cr: Distance upstream from next disturbance, inches 57" p: Distance downstream from last distubance, inches 7: Distance of Sample Level to Ground, feet 454u 65' A: Stack Inside Diameter, inches Estimated Moisture, percent Estimated Temperature, T l6' 0-2% 125 Estimated Velocity, fpm 1,400 Number of Ports 2 Figure l. Facility Schematic Representation i:i ii::: Ii i__ ! -:'.. :' qe/s/f a r :'l { I I I I 'j'I,l F1 rl rtlrl I -.!,li -tl,I 5"5;'s 2t!A --g's aht, E^1, -f 'j 4 o: 6.t,d) Ql,.'!|,?) €o:fl dv >'tott (;!.4art/r/ e0 ,oee/ b"7 E l-J iJ ti L L L t L- L t t LJ t LJ ll t L I':,- APPENDIX E Calibration of the console dry gas meter(s), pitottubes,lszzles diameters' andtemperature sensors were carried out in accordance with ti; irocedures ouflined in the auahty Assurance Handbook. The appropriate caribration Jata are iresented in the fonowing pages. The nozzle calibration, *, *,*d.d o'' the first page of the field data sheets. Figrre 3. Schematic of Method5lll4 Sampling Train Miter Box catibration Data and calculations Forms Post-test Dry Gas Meter Calibration Data Forms TYPe S Pitot Tube InsPection Data ' Sampte Box Temperature Sensor Calibration t( " .:,' .. lnpinger Train Sional; lvb/ Be Redaced . ByAl EqLt\Elont Cffinsir Tonoerall SensorTenpersfixre Sorsor,/IA-_\ ! /lTypssPitotfo. \ Sbck v1HGooseneck Nlo?do' \\ l-bgtTracsd classliud Prabe Tenpsratra* Sensors EnTty SSca C€l Ar-Trght runp TenpsreMo lnprpsrs lvbnonElbf Gass Ftltsr lbHar HeedArea iiii iIt lil*$l[ -lil Dryess tvbbr J' FTGURE 3 . . scnnl,raTrc RErRESENTATToN or Tiffi OD',;{SAMPLING TRAIN METHOD 5 DRY GAS METER CALTBRATION USING CRITTCAL ORIFICES 1) 2',) 3) 4) select three criticar orificgc to csribrate the dry gar mctcr which brad(.t thc exp.cld op€raung range,Record baromctic prcaeuru bcforc and aftor calibration proc.durc. Run at tc8ted vacuum (fiom Odltca Calibra{on Rcpo.t), ,or a p.riod of timcnecassary to achisvs a mlnlmum totel voluma of S cublc fc€tR€cord data and Intormadon in thc GREEN cells, yELLOW ccils ar€ calculatod. ilETER SER|{Lr: CRIIICAL ORIFICE SET SERIAL TI BAROMETRIC PRESSURE {In H EQUIPIENT lD I: l;;t AVG (Pb) 26.37 IF Y VARIATION EXCEEDS AOO%, ORIRGE SHOULD BE RECALIBRATED ENVIRONMENTAL SUPPLY COMPANY 293-/tl5 298.41r 2s8,4tg 303-az! 303.420 ,@.a22 l-';l rmF=r:lt6 lI I s lo.stzl ro I , I;'Fqflsl.f;r .',r | | s lo.srrzl ro I 5,OOl 5.001 5.002 5.461 6.006 t 0060 5.qX 5.003 t,oo8 USI}IG TI{E CruNCAI ORIFICES AS CAUBRATION STA}IDARDS: ThE foflqfllng oquauons ar€ usod b carcurab th€ standad wrumas of ak pass€d utrough he DGM, v. (sd), and 0lo qtbdodlbo, v' (su)' ard tre DGM calbrabn fador, y. Thaso oquatons * ,rorrt .ry..bur.ua i, u,. ,pr..orr,J.ur.. l/r\"at = K t t yn r P fur + L H I 13'6) tm vcrutt = *n "u{'?{ IAMD ' N€t volurns of gas sampre passcd through DGM, concd.d to standard conditionstq . 17.64 cR/in. Hg (E €tish), O.3SSO cK/mm H9 Uotric) Td t Ablolute DGM evg. teinperetura fR . Englbh, ol( - Mctric) s volumc of gas s.mPl€ Passcd thrugh the critlcal orlflco, @ncctod to standard condiuon3Td . AbrohJi. .||*icnt tcmp€ratr€ (h - Engilsh,1( _ t\r€fic) K I Av.rage K @orfiom Crl{c.l Orif,c. Csllbrsilonr DGM callbraUon faclor &s.14 314,885 3t'l.CE5 310.E 1 319.tsl 324"897 325.3700 330.371 330,371 335.374 335.374 340.3E2 79.75 80.75 82 83,00 84.75 85.25 86.25 85.75 88,25 !L1C81 4.1E78 tlIg. ,J€gS 4.1660 4.112A AvG. 4.51EO 4.56E5 112E3 4.1751 4.1246 4.1516 1.001 o.999 0.094 0.89E 1.01 I 1.o11 1.007 AVG! t.ol! 4.1119 4.119E 1.002 4"logs ,t 116l t.OO2 4,0951 4,1231 t.(X)? AVcr 1.003 0.60 (1) (21 Tomperaturo Eensors Rofergncc lnoF oFY =Yctu,,Yfru^ Out "F 3'l 77 114 31 76 '114 30n 113 5E 8t 83 n 78 68 a2 84 78 79 68 u 63 fs 60 MHl--" I f;l 1.83 LS! 1.A2r.'']EI-lLl F,s-lI z.oz I I r.rz I 1.51 r.g1 1,51F T[--llLI l__!41__lI rr.2o | | o.lt I AVERAGE DRY GAS METER .AL,BRATION FACTOR, ". @ AVEMGE AHn =l-:i:5,ls-l Alta- / o.zs e \' ox /5tgil\v_(srdl,, \ v. / {.57 1.42 1,12 1.11 6E t5 Ef 79 8t 68 a7 E9 81 82 3E 8E 90 EI 82 88 69 0t ut 8t 68 e0 92 80 81 EE e2 95 a2 u (3) METHOD 5 DRY GAS METER CALIBMTION USING CRITICAL ORIFICES 1 ) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range 2) Record barometric pressure before and afier calibration procedure. 3i Run at tested vacuum (from Orifics Calibration Report), for a Period of time necessary to achieve a minimum total volume of 5 cubic feet' 4) Record data and information in the GREEN cells, YELLOW cells are calculated' METER SERIAL CRITICAL ORIFICE SET SERIAL BAROMETRIC PRESSURE EQUIPMENT ID #: Facility FINALt;;I lnternational Uranium-North Yellowcake Dryer Scrubber AVG (Pu) 25.56 IF Y VARIATION EXCEEOS 2.OO%, ORIFICE SHOULD BE RECALIERATED I Ii ENVIRONMENTAL SUPPLY COMPANY ELAPSED TrME (MrN) U TESTED VACUUM (in Hs) 685,610 690;691 690.591 695.7i2 695.712 700.719 71 83 85 73 74 t2 a4 89 74 77 73 89 91 78 a2 , l;;T;;lI zg l.lo,.ro, I t, I| | . r,.,.,T1;ln:ffi'r-T-ll_l :i--r-l 5.08r 5.02't 5.007 78.75 81 85 0.00 0.00 0.00 0.00 0.00 0.00 le! 1.53 1.52 .0 .0 ,0 .0 ,0 .0 0.00 AVG = AVG' USTNG THE CRITICAL ORIFICES AS CALIBMTION STANDARDS: Th€ following equations are used to calculate the standard volumes of air passed through the DGM, V' (std), and the critical orifice, v., (std), and the DGM calibration factor, Y. These equations are automatically .. Pbar+(LH 113.6)Ym(,td)=Kt*rmt- f^ AVEMGE DRY GAs MErER cALrBRArroN FAcroR, " = [T66'il AVERAGEoT.=El (1) (21 AH6= ("ffi,)'*("#) Pbar * @Yqt"d.t = L*----=i lamD ,, vrru,r, I =-Vm@d\ I s.es | | t.as | 4.2774 9& 1.oogr:-----''lI g.sz I I t.as | 49,93 tM o'eeer--lI s.sz I I r.ss | 4.i667 4.161E 9€99 AVG = 1.001EFt=t= EF- = Net volume of gas sample passed through DGM, corrected to standard conditions K = 17.64'R/in Hg (English), 0 385E "Kmm Hg (Melrlc) T. = Absoluta DGM avg. t€mperstur€ ("R - English, "K ' Metric) = Volume of gas sample paised through the critical orifice, mrrected to standard conditions T@ = Absolute ambisnt temperatur€ (oR - English, "K ' Metric) K = Average K factor from Critical Orifi6 Calibration (3)E DGM calibration factor Console #5 Calibration METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) 2l 3) Sslcct thr€o critical oritices to calibrete tho dry gas m€t€r whlch bracket thc cxpecled oPgrating renge. Rccord baromctric prc$urc bcfoF and eftar celibration proccdura. Run at tected vacuum (from Orillca Calibretion Roport), tor . perlod of timo nccrs3ary to achievc a minlmum total volume of 5 cubic foct. Rrcord data and intormation in thc GREEN cells, YELLOW colls arc calculated. BAROMETRIC PRESSURE EOUIPMENT ID #: 4) DATE: METER PART T: Facllihr Internatlonal Uranlum'HorthYellowcake DryerBaghouse fffi;il AVG (Pb) 25.56 IF YVARIATION EXCEEDS 2.OO%, ORIFICE SHOULO BE RECALIBRATED IY ENVIRONMENTAL SUPPLY COMPANY IN]TIAL itaii:i }{l !iiilli!ttf!5crl 83, :rul ,,il'i ,i.,:; i !i:riiaa;l rriiEa :t:rl ii,lli'i:,,rid',1::,:::m: r i i3l ril lTl , mT;llfl:ffi t.019 5,014 5.011 .0 .0 .0 8E.zs fffj |lil 4.,'BEE 1r.€ eo.o ffi|@| 41416 4.tt43 os.5 | +ll;:,1 | z.zo | {fl.e! %"=ilrffi| '','l :hrffi H:ffi 0,00 0.00 0.00 0,00 0.00 0,00 tOl,gl:1li:; tiE:830, 711.W ,,::,?lGtlf ,lllir i ri ii:l;li! USING THE CRITICAL ORIFICES AS CALIBMTION STANDARDS: Thr tollou/ino rquations Br. u3cd to calculat tho slendard volum$ of air Patsed through thc DGM, Vm (std), and th. critic€l orillcc, Vq (std), and trc DGM calibration factor, Y. Th6sc cquations aro automstically 0.996 0.993 0.995 0.9e5 9,99 AvERAGE ORY GAS METER CALIBMTION FACTOR, '= @I AVERAGEAHe.FEI !E! lEc lJz AVG r vm(,d\ = lr tY^' Pbar +(LH 113'6) (rl \r'g' Tm vcr,--, = *', Pbar * @ ^lTanb ,, vrru,r, I =-Vntgd\ AHe' (ffi,I *(*i'j') (2) [:,],1 li',::l.l;': .0 .0 .0 ffiffi ffiE r Nat volums of gas sampl€ pasaed through DGM, corrected to standard conditiong 6 = 17.64 "Mn. Hg (English), 0.3858 "K/mm Hg (Mstrlc) Tn - Absolute OGM avg. temPeratur€ fR ' Engllsh' oK ' Metric) . volumc ot ga3 3amplc pa$cd through tho critical orlfic., concctsd to 3tendard condition3 Td o Ab3olute ambiEnt temPeretute ("R - Engli3h, oK ' Msiric) K ' Avcng€ K fado. trom Criticel Orttic. Callbetlon illi:rl.:i:il,i (3). DGM calibreuon factor Con3ola #5 Calibratlon Type S Pitot Tube Inspection Data . . Pitot'l\rbe ldcntificarion : J*7 - Q Tcchnician: Kn.^.6^ Cor, I t D= ,77l_ln. Ps= .'l Ll I m. Is Pn=Ps? V Is 1.05:D, S Q <.1.50,Dr? / cs < l0o dt ='.o -:' a2 < lQ9 9rf5o Fz<5t Fz- e^= ,19[ in. c.rl" o- I oPt- __!_- H. o I p-z Zs0.125in. W < 0.03 125 in .o33z= w=t6 tn. The pitot tubc mccts thc spccifications for a calibratio faaor of 0-&4? t/ Type S Pitot Tube In3pection Data ?c_a- . :: PitotTubcldentification: Jo - sl D,=,3?f i". 3'tz Pg O1 Is Is 1.05.D,SD,3 cr1 < l0o--TI cq < l0o Q 2<oPl'-J -l .j 9t=... O | ' _.O,o1. ir,. I I Fr{5o 2s0..125 in" .. : . : Ws 0.03125 in. I The pitot tubc mccts the qpecificatiors for s calibration factor of0.8 4? \/ pr- - </>7 Pa- Pr=Ps ?' V'1.50..Dt? ,/a o,-. ./ .' .z= tn. u. ' Sample Box Temperature Sensor Calibration Date: /l 4 A -Ofralibrator:,A Kth/,-,Referencc: ,r/f:f Unit ID Temperafure Difference cF) C fn APPENDIX F The testing protocol and other correspondence related to the tests are included here' I SEMI.AI\NUAL EMISSION TESTING PROTOCOL FOR RADIONUCLIDE PARTICULATE MATTER AT INTERNATIONAL URANIUM (USA) CORPORATION BLANDING' UTAH YELLOW CAKE NORTH DRYER SCRUBBER YELLOW CAKE DRYER BAGHOUSE August 30,2006 Project Organization and Responsibility The following personnel and the testing contractor are presently anticipated to be involved in the testin! program. The Utah Department of Environmental Quality, Division of Air euality (DAe) *a gpa may have their own personnel to observe all phases including the process. Company Contacts International Uranium (USA) Corporation Wally Brice 435-678-2221 P.O. Box 809 Blanding, Utah 84511 TETCO Dean Kitchen 801-768-0973 90 East Main Paul R' Kitchen Lehi, Utah 84043 Facility and Location International Uranium's White Mesa Mill is located 6 miles south of Blanding, Utah on Highway 191. The Mill processes uranium ore. There are two yellow cake dryers with individual scrubbers but only the Yellow Cake North Dryer is currently in operation and will.be tested. The Yellow Cake Dryer Baghouse serves the dryer enclosure and hopper' Test Obiective These test will be conducted to measure the radionucleide emissions on the scrubber and baghouse that serves the Yellow Cake ore processing operation at the facility. Testing prJ"ed*"s will include accumulating pto.its and production data as well as testing for Radionucleide emissions using EPA Method 5lll4' Test Schedule Testing will follow this protocol for the fourth quarter of 2006 and the second and fourth quarters of zool. Testing in the fourth quarter of 2006 is scheduled for october 17'19'2006' Notification of test datesln other quarteis will be sent as they are scheduled by the facility. Site Access The sample sites are located on the building roof and are accessed by stairs and ladders inside the building. Potential Hazards Moving EquiPment - Yes Hot EquiPment - Yes Chemical - Yes Other - Radioactive Process Data All operational and instrumentation data will be made available to DAQ personnel' The facility will run at normal conditions. Ouality Assurance All testing and analysis in these tests will be conducted according to EPA Methods 5lll4' 2 Reporting ReportingwillbepreparedbyJhetestingcontractoraccordingtoEPAQualrtyAssurance Guidelines. A complete copy of raw data and trst carculatiorr, ,**y will be included in the reports. All process *a proirr",io" 11i will be recorded by International Uranium (USA) p.'rro*.f foi inspection fy DAQ and EPA' if requested' Test Procedures Radionuclideemissiontestingwillbeconductedonthescrubberandbaghouseexhaust stacksaccording,ogpaMethod5l||4.SpecificproceduresareaSfollows: l. The sample locations and the number of sample points will comply with the requirements of EPA Method 1' TheinsidediameteroftheYellowCakeNorthDryerScrubberstackexhaustislsinches. Theportsarelocatedll4inches(6.3diameters)upstreamfromthenextdisturbanceand 114 inches tz: Jiu-.ters) downstream from the last disturbance. The inside diameter of the yellow cake Dryer Baghouse stack is 16'0 inches' The two' four-inchdiametersampleportruretocated28'3Sdiameters(454inches)downstream from the last disturbance and gSi diameters (57 inches) upstream from the next disturbance. 2. EpA Method 2 will be used to determine the gas stream velocity. Type "S" pitot tubes will be used with a Co factor of oi+. pual inilined/vertical manometers with graduations of 0.01 inches of water will be used. If the flows are below '25 inches of water a more sensitivemanometerwillbe,,,"a.rr'"graduationmarksonitare.005inchesofwater. Direction ;i;;; fil* will be ri""t"a roi gas cyclonics prior to testing' If the average deviation is over 20 degrees, th"n straightening,,*"' will be installed or other arrangements agreeable to DAQ will be made' 3. Test run time will be at least 60 minutes for each test run 4.EPAMethod3willbeusedtodeterminethegasstreamdrymolecularweightifthe exhaust gas is not ambient. An integrated flui gas sample will be tlken from the exhaust lineafterthedrygasmeterorificea*i"geachtestrunandanalyzedatthecompletionof the test with an orsat to determine the rnolecular weight of the effluent gas stream' If the exhaustgasisambientairthenTETCOwilluseadry-molecularweightof23.84lb/lbmol (20-9 percent Or, 79'1 percent N,) in all calculations' 5. EPA Method 4 will be followed to determine the gas stream moisture content' 7. 8. Probe liners will be 316 stainless steel for all tests' The glass fiber filters used will meet the requirements of EPA Method 5lll4' The barometric pressure will be measured with a barometer which is periodically checked uguirrrt a mercury barometer. The barometer will be checked prior to testing to assure an accurate barometric Pressure' All current calibration data is submitted with this protocol, exceptnozzle calibration which will be done at the test site. Nozzle calibraiion will be included on the first page of each set of run sheets for each respective test run. Any calibration that is not current will be re-calibrated prior to the test dates' Any necessary preparation and clean-up by the contractor will be performed in the contractor's ,u.ptittg trailer or a clean area on lntemational Uranium's property' Laboratory work anianalysis will be completed by the contractor and Energy Laboratories as soon as possible after the test project' Verbal results will be reported to Wally Brice of lnternational Uranium (USA)' The written report will follow within 30 days following the completion of the test' If maintenance or operating problems arise during the test, the test may be stopped' This deterrnination will u" *uaJiy Intemational Uranium (USA) representatives and op"ruting personnel in consultation with DAQ representatives 9. 10. ll. 12. Estimates of Test Parameters The values estimates onlY and below are estimates of the stack flow rates and temperatures- These are are not intended to reflect permitted values' Temperature oF Velocity fom Moisture % Yellow Cake Dryer Scrubber Varies 70-125 dePending on weather and time of Year' I 100 Near Saturation Yellow Cake Dryer Baghouse ll5 1300 I Appendix A Facility Schematics Yellow Cake North Dryer Scrubber Yellow Cake DrYer Baghouse Inte rtnati onal UraniumFacility: Stack rdentincation: North Yellow Cake Scrubber a: Distance upsteam from next disturbance, feet p: Distance downsteam from last disturbance, feet y: Distance of Sample Level to floor, feet @: Stacklnside Diameter, inches Estimated Moisture, Percent Estimated TemPerature, T Estimated VelocitY, Sm Number of Ports 9.5' 9.5' 65' 18" Near Saturation 70-125 1.100 l+a+l Control Unit Type:Yellow Cake Processing t ct ,f Figure 1. Facility Schematic Representation Faci,i,y: InterTrational lJranium Stack tdentifi."r,""' B aghOUSe 1+a+l cr: Distance upsr:am from next disturbance' inches p: Distance downstream from last disturbance' inches 1: Distance of Sample Level to Ground' feet O: Stack Inside Diameter, inches Estimated Moisture, Percent Estimated TemPerature, oF Estimated VelocitY, fPm Number of Ports 57" 454" 65' 16" 0-2% 125 1.400 Figure l. Facility Schematic Representation Appendix B Calibration Data METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three cntical orifices to calibrate the dry gas meter which bracket the expected operating range 2) Record barometric pressure before and after calibration Prooedure. 3) Run at tested vacuum (from Onfice Calibration Report), for a Period of tlme necessary to achieve a minimum total volume of 5 oubic feet. 4) Record data and information in the GREEN oells, YELLOW cells are calculated. BAROMETRIC PRESSURE EOUIPMENT IO 'T Facility FINALtffilI '6,39 "1 New Callbratlon AVG (Pbr) 25.39DATE: METER PART 'T IF Y VARIATION EXCEEDS 2.OO%, ORIFICE SHOULD BE RECALIBRATED IIt ENVIRONMENTAL SUPPLY COMPANY 88120i6::j::il isz,i5o,. i d*oitl"" 905.1'9 .:rlS::r:r:li 'l:.:toi:ri t*91,,,:lrr81.ir B3 ':::ltit::;i; ::r:9!l:i::: ::ii::i::::ril ;:BB:: ::l::::::|:::;l:::tt A3l 83,i,88::::::::llr'd!::ri:s$:i.:t6 l .--Tl ,[:m l', 30,lz lo.e'ri,ffiI '''''l . lAr-.+tr'El lTl ,l;,milIrsl,|...El ';l| | 3 10.53{7f 13, I i.3t5i i,ao, 5t99 | ti24i: 'q'910,:52E9, alog' '1210 r.208 83 ffiHe+: | l-,?.!i'ler:u l -rbi I l,','?.es I ,,* llJill |r;ll ;,.ru [ETlo.,. lTbf |T-.;1 tT::-11Blr.oo I ii.tt I I on6 B4.bs t,il+., | | :o.le',,1 B4,so I t2.00 ll 0;461 AvERAGE DRy GAs METER cALtBFATtoN FAcroR, " = @l AVERAGEAHs=t.:.'.:iFl AHq= (ffi)'^"(ry) 4.4489: #,nitot 'r. -'4.m07::T ,4:3566 +ry t.?390 4,2920 4.4U3 Q.997 : '' Is€e 9€914try$ , ry, avc = . 0.996:::..']::.ga3 ry 9-* 1j99 4.3583 l49SAvG- +ry4,2311 j4g 4.s,272 1g 4.a?62 +EgC, AVG . 1:009 {.63 4.04 s€g lJgr 1{E. lJt 4, lfc 'l:8C lg 1:64 1.64 USING THE CRNICAL ORIFTCES AS CALIBMTION STANDARDS: Tho ldowing equalions 6re ussd to cdcrtato th6 olanddd vdumes of ai pass€d thro{jgh the DGM, Vm (sld), and lho crilicd orifica, Vo (std), and tho DGM cdibration faclor, Y. Thesc equalions ae automalicdy cdculated in tho Wroadsheet above Fl;mI 'l s lo.g3orl tg.l (1) Vmruo, = Kr*r^*'-!tffM ,.,. Pbo *@lq,at = I-,--- J ra'nD ,, Vcr@d)t =;_/fr@lt (21 905a0 :lltOi388 'rr.::.r:: , 9,16,3ht,,qll::AqE 9'15:!95:,:'920.806, =Netvo|umeofgassamp|ePassedthroughDGM,correctedtostandardconditions K1 = 17.64 oR./in. Hg (English), 0 3858 "Kmm Hg (Metrlc) Tm = Absotule OGM avg, tsmpelaturc CR ' English' "K ' Metric) = volume of gas sample passed through the critical orifice, corrected to standard conditions Td : Ab6olute ambisnt temperature fR ' English, oK ' Mskic) K = Awrago K factor from Critical Orifioo Calibtation ,ct5.LS ',Citid4$ci6.liic FB0:6rg :e85:992,: .80 :::a:N 82. tfi tKl::: l .t:'g:..]::: c':::s2 '::,,bo-,i a ,,,86 a2 ,1,62', *t ff ::81 g5 h3 86i, : r.::itt rgdr::r tll::i ul trs 85,85::r:,8i1:84 (3)= DGM calibration factor Console #3 Calibration METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) 2', J' Select three critical orific€s to calibrate th6 dry gas metar which bracket the expec{ed operating range. Rrcord barometric pressurc bolors and aftcr calibratlon prgccdura. Run at tsstcd vecuum (from Orifico Calibration RePort), for a p€dod of time neceseary to echieve e minlmum total volumo of 5 cubic fcct. RGcord data and information in the GREEN cells, YELLOW c€lls are celculated' BAROMETRIC PRESSURE (ln H EQUIPMENT ID #: 4) DATE: METER PART #: FINALfr.-;l AVG (Pt.l 25.52 IF Y VARIANON EXCEEPS 2'OO%' ORIFICE SHOULD BE RECALIBRATEO i INITIAL ELAPSED TIME (MlN) e 832.834 E3E.009 838.009 84:t.t04 c4:i,'104 E46.30E E9 74 71 7E 83 83 71 73 7a n 69 73 73 7a 80 l-l , [;T;I ro I,l'""'F'lr I o.ersz I ts I l-l ' lor"T *-l| ,tt | .lo.""l " I| | 3 10.53171 ro I Vmlrat= Xr*Yr'Ag#M Vcrr,,at = K" Pbg '?! lan'O Y =V,,,U,!Vmr,ut E4E.308 853.761 853.761 858.903 8t8.003 E64.081 5.176 5,095 5,204 5.453 5.142 5.151 n,25 75 76 76,50 76.75 76.75 76.50 78,00 76.25 t--r I f.; f.--''_-l t-*lf;l t-,.;l r,--;l r.';l Iz.rtIIt.'lIr;,-l l;l r*-;l r,;r'.;l-,;t-,.; r;l AvEMGE DRY GAs METER cALIBRATION FACTOR, Y = Ij.J...ffiI AVERAGE aH. =17.50-l Tomperaturo S€naora Referonce In OF 32 32 83 82 !,3700 1.t212 4.4054 L!031 4,3291 {-33er 4,3240 4.3112 43!C4 laEg 9,9CC 4,2189 gJgl !n@ 9€95 AVG r 0'985 4.5709 0.995 4.ze7e gJC! 4.2eoo 0p9SAVG= qggl 4g!-91 o.ses /t.3079 0,999 !|@ 0.e9e avc= EE -o.72 0.05 9.92 1.49 1.49 ue 1.5.1 1.54 L9! 1.48 l,tlC 1.48|*lrffiI I ' l.,r'T,, I 5,1.14 5,121 5.123 804.0540 869.196 869.'t98 871,322 E71.t22 870.44{t USING TI{E CRITICAL ORIFICES AS CALIBRATION STAilDARDS: The followtng equations a19 used to calcuhts ths standard \olu.nss of air Pass€d htough ths DGM, Vn (std)' and ths crithal orillco, Vo (std), ard he OGM calibralion facior, Y. Thosd oqualions aI8 automathally €bulat€d in ho spcadsheot abow. Out 32 83 118 (11 (2) = Net volum€ of gas eample passed through DGM, conected to standard conditions Kl = 17,04 oRiln. Hg (Englieh), 0.3858 oK/mm Hg (Motric) T. = Abrolute OGM avg. tomPoreture (oR - English' oK - Mctric) : volumc qf gaE sample passed through the crlticel orifico, conec{ed to standard conditions Td = Ablotute ambient temFrature (oR ' English, oK - Mstric) K = Avorago K tecio( trom Criticel Otifico C'llbration AHa= ("ffi,)'*(Y) 69 73 71 7g 80 69 74 f1 fg 80 70 73 f1 7g 81 70 74 76 79 7E 70 fl 75 78 Tf f1 76 76 n 7a (3)! DGM celibration taclol 119 tte Console tA Calibration i:=3J'E+ METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1 ) select three critical orifices to calibrate the dry gas meter which brackot the exp.cted oporatlng range 2) Record barometric pressure before and after calibration proceduro' 3) Run at tosted vacuum (from Orifico Calibration RePort), for a Pcriod of time nec€ssary to achievs a minimum total volume of 5 cubic feot' 4) Record data and information in the GREEN c6ll8, YELLOW c6lls are calculatod' DATE:METER SERIAL CR]TICAL ORIFICE SET SERIAL BAROMETRTC PRESSUBE]b-E EQUIPMENT ID fl: trtrtr r;T;]lrr"tT;|;;T;-l I.r"tT;ffiT;]l'-rTT._l r.,*'T;ffiT;']l'"trT; 1 2 3 1 2 3 t 2 3 USING T}IE CRITICAL ORIFICES AS CALIBRATIOII STAilDARDS: The following equations are used to calfllate tho standad volumss ol air passed though m OGM, V. (std), and the cdtlcal orifrce, v, (std), and ho DGM calibrathn factor, Y. These equations ar€ automatlcally cabulated in he spcadshoEt abovo' ,, Pbar+(M 113.6)lttt\sut= Lr*Ym'- Vcr,,n,, = K'. Pb{ " ?! taT ) ,. l/crrur,l=-rmttt,t\ 293.416 298.419 298.'ft9 303.420 303,420 30s.122 309J24 3tr1,885 314,E86 310.E91 319.891 324.897 325.3700 330.37'l 330.371 335.374 335.374 340.382 = N€t volume of ga3 samPle passed through OGM' conected to standard conditions Kr : 17.64 orUin Hg (English)' 0'3858 "Kmm Hg (Metric) T. = Absolute DGM avg tonperature (oR ' Engllsh' oK - Mctdc) !Vo|umoofgagsamPtepasgedthroughthccriti6|ori'i^co.cor€ctedtostandardconditions T* = Ab*|.,t" "tbisnt temP€rature (oR ' En€lilh' 1( - Mcitic) K = Avcrage K faclor from Crlticel Orifica Callbration Temporature Senaors Reference lnoF oF aHa = I o.zs e 1' ax (hFg\\v..(std),, \ v.,, tF Y VARIATION EXCEEDS 2'Oo%' ORIFICE S}IOULD BE RECALIBRATED I * FINALr,;AVG (Pr) 25.r7 5.004 5.001 6.002 5.461 5,000 6.0060 5.001 5.003 6.008 ?9.75 80.75 82 83.00 8.1.75 85.25 85.25 E5,75 88.25 4.185'l t11& 1J.@ 4.5180 .1.t283 1.1215 4.11 19 4.1098 4g! 4JCZ! 1=9!lL 4,'1698 0.999 alg 0.ee4 AVGg 0.988 4,59S 1'011 1.1751 M1 4llill! usz AVG = t.010 4.1198 :ge 4.,t.r51 193 t1234 1.007 AVG= 1.003 g5r 9S .o.02 1.83 l,9it 1.42 1.51 L!1 t!1 1.4? LE EI OutoF 31 114 (1) l2l al 76 114 an 77 113 INMAL METER PART #: 68 8t 8:t fl 78 6E a2 84 78 79 CE u 8E 7A EO t-a-l 1-_l'trtt--r.14 t-gtI z.oz I | 1.12 |r;IE !:;z-l l-sr-]I rr.ze I I 0.41 I AVERAGE DRY GAs MErER cALlBRArloN FAcroR' " " [@l AVERAGEot"=@l 68 85 a7 79 8t 08 87 89 8't E2 68 88 90 8t 82 88 89 91 80 81 6E 90 02 80 E1 08 92 96 a2 84 (31 r OGM calibration taoior Console #5 Calibration METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1 ) Select thre€ critical orifices to calibrate the dry gas moter which bracket the expected operating range' 2) Record barometric pressure before and aftercalibralion procedure. 3) Run al lesled vacuum (from Orifico Calibration Report), for a Poriod of lime necossary lo achieve e minimum tolal volume of 5 oubio feot. 4) Record data end informalion in the GREEN cells, YELLOW cells are calculaled. BAROMETRIC PRESSURE EAUIPMENT ID f: FINALfiffil AVO lPFl 25.70 IF Y VARIATION EXCEEDS 2.OO%' ORIFICE SHOULD BE RECALIBRATED I Y ENVIRONMENTAL SUPPLY COMPANY INITIAL ELAPSED TIME (MIN e TESTEO vacuuM lln Hs) ,,,:tloi:lxi$e,lrio l ,.6,13.'60 Gieitdiittt, 619t17.:.:.i;iriieri.iiitit t5:::t,1 tltlrf,5 35i,,r::E$:i:l .:::!t03 : ::85 TF ,ioi :, .,,lsi,i 86..:t::,li:ii:il :,10{:iioi;. ITt , [iliilllilllrol,ml' I c I o.arsr,l re I I-1 ,'i;ilIt.,'t]|"'c|'FETTII I 3 lo53{71 ie I 9rls . S.S,l7:: t.69t stis' 'Ci+1 rssit :: :5^ot5 :::l:5.079 :s3st 921fs, 93,29, :91ii:l , li,rc I 901Ii ,9i!.00 :l'': "77'l,i , ai;oo . s5:oo 4+63?8 ff:4;7092 trs9, +sdib t.zt4i'ry ,taps !.,6lli!!-, 4d!9: :&4:,' AVG E l,a*g1,.. 1i31ql ' ,c$it AVG = !.??q7 ' LZSIO 4.4894 AVG = s4c -0.0? .ti/il 49., !rylg: t.007g ir.igg' 1.005 r.ooz ,opl7i 0.998 t.001 ,0.99s USING THE CRITICAL ORIFICES AS CALIBRATION STANOAROS: The folbriving equalions ar€ used to cabuHe the slandsrd \olmes of dr Pas6ed thrqrgh tre DGM' V. (sld), md the critbalorifice' vd (s1d), ald th€ oGM caibration fator, Y. Thsso oquations afe aJlomElicaly cabubled in the spresdsheet 8bo,B' (1) vtnlaat = *,*r**!!!i#M .-,. Pbar * @ / w. (rd\ - 't t=----- "'l I amD ,, V"ru,o, I =-v^'no' 573:,lil3 578:140 s78:rlo (et:t g:: 583219 588:f,16 1 =Nelvo|um€ofgassamp|epassedthroughDGM,conectedtoslandardconditions K' = 17 64 "R/in. Hg (English), 0 3858 "l(mm Hg (Metric) T, = Absolute DGM avg. temp€ratur€ ("R - English' "K - Metric) = Volume of gas sample passed through the crilical orifice, corrected lo siandard condilions Td = AbsolutE ambient tomp€rature ("R - English. "K - Metric) K = Awrage K bctor from Critical Orifice Calibration OutoF 34 bo 120 (2) oF ot 1)1 OF 34 bo 120 rffil H l :i::d.;'. '1 l, rto.,ItlEill l-:':'J-Tfffiffih#ffiffiHl, ii.sr" I I' ore IlrEtlt._;;'l AVERAGE DRY GAs METERcALIBRATIoN FAcTOR,'= E@l AVERAGEAHq=Fm] AHq = / o.zs e \' ox lUCgt\\v"l",al/ \ ", i Temperature Sensors Reference In :::595;mg COB::nqC .;an.J;' coo,C,l7 .:: t:l::...r: i: 006;tlq,,,: .,::#:r.r:.rr E6: .r::1:t t1: :.1::;92: ]',',,,,,if :;:::t6::i:r1:r::l...i8{.i,iil ,. 'S5,,: .96:::r:l 1,,.6.,... to ,,l.Ft,il:!5,'.ir::::':::::: i9l',,, l.tO,,,t4 75 :,1 :).:lA:t:tl 8rt :76 73 ?6::::l I. i:; :: I ',':0$,87: tn BO :l:::E3 87'S2, (3)= DGM calibration factor Console #6 Calibration Dale: D, Type S Pitot Tube lnspection Data ; . ' Pitot Tube ldcntification: Z7i. I r""a^"i^,.: Q ou., O l9-^ I R -<-'r^.U,^T --4 E J fr \_ D,= -Z5o in. ea- 33Lf ;n. yr= 3j4 i". Is Pe=Ps? vl Is 1.05. D, S D, < 1.50'Dr? y' d1 < l0o ct:' c2 < l0o t 9r55o z 9r= 9z<5o 9z:2" 4-Z 230.125 in.7= .O./ O in. W<0.03125 in.w: The pitot tube meets the specifications for a calibration factor of0.84? Reference: O1 Q2 foIpr 92 - oo3 ln. 'l'emperature Differencc t/,Date;-@N:-D, I/ --'fl-;l e , 4o' - Yp2 The pitot tube meets the specifications for a calibration factor of0.84? J Refercntp: d1 < l0o o,=---L-o -'- '': Type S Pitot Tube Inspection Data . fs Pa:Ps? Is 1.05 . D, ( Dt < I.50'Dr ? o2 < l0o FrS5' 9r<5o PitotTubeldentification: Z'7 - Z q: Z JiD in. P^= 3 fO in. P"=_.)f9_in. Ffo' z=.0)8;n' 2- Fz: Tempcraturc Difference z : Type S Pitot Tube Inspection Data : PitotTubcldentification: ar r: rccuician: K-e ^rGn Cors PitotTubcldentification: )-7 - A Dr=,7-7f ,'l4l H: ls Is 1.05.D, S D,3. a2 < 10" FrS5o 9:<5o 9r=t1L,' *-z Zs0.l25il., W < 0.03125 itt f The pitot tubc meets lhc spccifications for a calibrarion factor of0.84? { Tcmocraturc Scosor Cdibration Refcrcncq P^= ,!ql Pa= Prr=Ps? V 1.50. Dr ? vl 01 < l0o c't:' :O o,=l' h=1" z= -O33 . i". *= .il6 ^- ln- m. m. nat": /V- 29 -&fnvl Type S PitotTubelnipection Data q= 2.n Pr= ss-1/ 36 -.e Is Is 1.05'D, < D, S cr1 < tOo c2 < l0o t 9rS5o Fr<5o v Z<0.125 in. Ws 0.03125 in. ln. n. g The pitot tubc meets thc spccilications for a calibration faclor of0.g4? T--!---!_ _ Tcmpcraturc Sarsor Calibraiion Rcferancc: z= .01{ ? i,. w= o^r", lZ-2? 'of, D, /T H Type S Piiot Tube IniPection Data .: D,= Pe= Ps= Pe=Pn ? ' t/ Pitot Tubc ldentifi cation:36- > zfa 3fv 3s-q ln, tn. m. Is D,3 C1 ctz Is 1.05'Q 3 l:50'D,'] - , .',=' O o cr1 < l0o ' o2< l0o : p1 f5o a,= J ' Fr= R-= lo F:<5o 230.125 in. W < 0.03125 in. - O:oL= . v-I m. 1ry= .Ol? iru Rcfcrcnce: g4q lz-L-/ -oS- fype S PitotTube Injpection Dita' - 7d /^. : :.: PitotTubeldentification: Jo - (al Is I.05.QS Tcchnician:" D,= ,37 t P^= .n>7 p,= 317 Pe=Ps ? Vt 1.50..D. ? { ln. tn. m. Is q< a2=Oo g'c1 < l0o d2 < l0o 9135"Fr= z= .oo1 tn. w= '07? i,'. Fr<5o +-z Zs0.125 in. :' W < 0.03 125 in. The pitot tube meets thc specifications for a cglibration factor of0.84? p2 rliluv Sample Box Temperature Sensor Calibration I I \ Datc: /) 4 A - A,tt7-alibraton 2 Kth/.-,Rcferencc: ,llf-:f UnitID Temperature Difference cn / C t- SiNCE H EUSSER NEWEIGH rgOE Certi/icate of B ulsnce Culibrution CustomirNami -leb'rtiacaitNa: -O66ltz Department:Calibration Date: January 12,2006,Address: 90 East Main St. lOrderNumber: :CitylstateliLip: Lehi, UT 84043 lTechnician: Mark B.Contactl Dean ;ProcedureUsed: WP-703 @ev.2002-1)..---'-- , Manufaciiiiei: *-Gnver iiiffiter;t-- ,Model: A.2.50 iX- Calibration: rldentification No. lX - Certification: Serial Number: 8045284 i Corrective Maintenance::Readability:0.0001gCapacity:250g;order(SeeComments): ---t { I II Next Calibration & Certification Due: January 12,2OOz Mass Standards Used for Calibration: Cal I.D. #45, CalI.D. #46, CaLI.D. #47 PRE-CALlBRATION POST-CALIBRATION Gomments: : Pertinent tnformation: The mass reference standards used tq calibrate and certify this mass measurement instument are taceable to the National lnstitute of Standards & Technologl (NIST) wilh an uncertainty less than or equal to % of the class tolerance. The procedure used to calibrate the herein described artifact and this Certificate of Balarce Calibration meets the requirements and guidelines of ISO 9001:2000, ISO Guide 25, ANSIA{CSL 2540-l-1994, the Heusser Neweigb Quality Assurance Prograd (Revision 2002- This is to certify the data reported herein is true and correct at the time of calibration/certification. HEUSSER NEWEIGH 1247 West Meadowbrook Lane, Lehi, UT 84043, (577)766-4492 This Certificate of Calibration shall not bc reproduced orccat in full, without the written tpproval of Heusser Newcigh. NominalMass Value lndicated Weight (s)Conection (g)lndicated , Weight (g)Correction (g)]ontrolLimit t, (g) Post-Cal. Within Confolj 'timit? 1 0.999s -0.0001 1.0001 0.0001 0.0005 Yes', 10 9.9997 -0.0003 0.0005 -Yes 20 20.0001 0.0001 0.0005 Yes, 50 49.9992 -0.0008 49.9995 -0.0005 0.0005 ':Yes to0 99.9996 -0.0004 100.0002 0.0002 0.0010 Yes 200 199.9985 -0.0015 199.9998 0.0002 0.0020'i Yes r ComDlete iterns 1,2, and'3' Also acmplete item 4 if Restricted Delivery is desired.-I Print yout name and address on the rcvqsd ;so thdt wb. can retun the calrd to you.r Atach this cand to the back of the mailplece'' oron'the frontJf space Permlts. C. Dat€ of Dolivery "ffiNTMM6W,,,EIT EI Agent tr 1. Artlcle Addressed to: R;cli,*J 37"o?+ UJ..h b*q :P,o . Bov ti487O 4ntf l-zKc e,q W 7\ilq'482o 3- "S€Ivlce TYPo F C€rtm€d Mall E Expr€ssMalt tl n"gb'td"d El Retum necetpt for: Metrchandlse Et Insurcd Mall E c'o.o. 4. Restlcted D€ft{af? (ErfaF6€,)E Yes 2. ,\rtlcla Number Gran$rhon selfu@,d)?0Brt -rl?stl t1801 Z3!3 w Ps Form 3811, February Domestlc Retum-Rec€lPt 1e2s9s{2-[fi1540 |