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HomeMy WebLinkAboutDRC-2005-001105 - 0901a06880805785I T t t I I T I I I I I I t I t I t I White Mesa Uranium Mill Groundwater and DMT Performance Standard Monitoring Report State of Utah Groundwater Discharge Permit No. UGW370004 l't Quarter (January through March) 2005 Prepared by: INTERNATIONAL URANIUM (USA) CORPORATION Suite g5o, l05o l Tth Street Denver CO 80265 June 30,2005 I I I t I I I I I I T I t I I I I I T 1. INTRODUCTION This is the Routine Groundwater Monitoring Report, as required under part I.F.l of Stateof Utah Groundwater"Discharge Permit No. :ZOOO4 (the "permit,,), and the Routine DMTPerformance Standard Monitoring Report, as required under Parl I.F.2 of the permit, forthe 1't quarter of 2005 (the "Quart"r;; fo. International Uranium (USA) Corporation,s("iUSA's") White Mesa Uranium Mill (the "Mi11"). This Report includes alifield andlaboratory analyses of all well monitoring and samples taken during the euarter, asrequired under Parts I.E.1, 1.8.2 and I.E.4 of the fermit and all DMT perfornance Standard monitoring results for the Quarter required under part I.E.6 of the permit. 2. GROUNDWATER MONITORING 2.1. Samples and Measurements Taken During the euarter During the Quarter, the foilor.ving groundwater samples and measurements were taken: a) Groundwater Compliance Monitoring Groundwater Compliance Monitoring was performed in downgradient wells MW-11,MW-14, MW-26 and MW-32, pursuant to Part I.E.1. a) of the Permit. These sampleswere analyzed for all parameters listed in Table 2 of the Permit; however, someparameters required_ by Parl LE.l.c)2)ii were inadvertently not analyzed. Thoseparameters were carbonate, bicarbonate, sodium, potassium, magnesium, calcium, andtotal anions and catious. Those analytes will be included in all future analvses. bl Croundwatct. Hcud Monitoring Depth to groundwater was taken in the following wells and,lorpiezometers, pursuant toParr I.8.2 of the Permit: (i) The poinr of compiiance welrs listed in paragraph 2.1.a) above;(ii) Piezometers - P-1, p-2,p-3, p-4 and p-5; (iii) Existing monitoring wells - MW-20 andMW_22; and(iv) All of the temporary chloroform investigation wells. 2.2. Field Data Sheets Attached under Tab A are copies of all field data sheets that were collected during the Quarter for the groundwater compliance monitoring wells listed in paragraph 2.1 (a)above, as well as for a field blank (MW-60) and a duplicate sample of Mw-l r iiraw-o:).Groundwater compliance monitoring during the Period *u. p..fo.*ed under the existinggroundwater sampling standard operating procedure ("SOP") and euality Assurance plan("QAP"). The field data sheets for the Quarter do not include all of the informationspecified in Part I.F-l.a) of the Permit, as required under the revised GroundwaterSampling Procedure and Quality Assurance Plan that are in the process of being I I I I I I I I I I t I t I I I I t I 1. INTRODUCTION This is the Routine Groundwater Monitoring Reporl, as required under Part I.F.l of State of Utah Groundwater Discharge Permit No. 370004 (the "Permit"), and the Routine DMT Performance Standard Monitoring Report, as required under PafiI.F.2 of the permit, for the l't quarter of 2005 (the "Quart"r;'; fo, Inteinational uranium (JSA) Corporation,s("IUSA's") White Mesa Uranium Mill (the "Mill"). This Report includes alf field and laboratory analyses of ali well monitoring and samples taken during the Quarter, as required under Parts I.E.7,I.8.2 and LE.4 of the Permit and all DMT Performance Standard monitoring results for the Quarter required under Part I.E.6 of the permit. 2. GROUNDWATERMONITORING 2.1. Samples and Measurements Taken During the euarter During the Quarter, the following groundwater samples and measurements were taken: ,) Groundwater Compliancc Monitoring Groundwater Compliance Monitoring was performed in downgradient wells MW-l1, MW-14, MW-26 and MW-32, pursuant to Part I.E.l. a) of the Permit. These sampleswere analyzed for ali parameters listed in Table 2 of the Permit; however, some parameters required by Parl I.E.l.c)2)ii were inadverlently not analyzed. Those parameters were carbonate, bicarbonate, sodium, potassium, magnesium, calcium, and total anions and cations. Those analltes will be included in all future analyses. b) Groundwatet'Hcad Monitoring Depth to groundwater was taken in the following weils and/or piezometers, pursuant toPartl.E.2 of the Pernrit: (i) The point of compliance wells listed in paragraph 2.1.a) above;(ii) Piezometers P-1, P-2,P-3, P-4 and p-5; (iii) Existing monitoring wells - MW-20 and MW-22; and(iv) All of the temporary chloroform investigation wells. 2.2. Field Data Sheets Attached under Tab A are copies of all field data sheets that were collected during the Quarter for the groundwater compliance monitoring wells listed in paragraph 2.1 (a) above, as well as for a field blank (MW-60) and a duplicare sample of MW-l r-gvtw-o:;. Groundwater compliance monitoring during the Period was performed under the existing groundwater sampling standard operating procedure ("SOP") and Quality Assurance plan ("QAP"). The field data sheets for the Quarter do not include all of the information specified in Parl I.F.l.a) of the Permit, as required under the revised Groundwater Sampling Procedure and Quality Assurance Plan that are in the process of being developed under Parl 1.H.6 of the Pennit. The revised draft SOp and eAp will beemployed by Mill personnel commencing with the 2"d quafier 2005 sampling. 2.3. Laboratory Results 2.3.1. Copy of Laboratoriz Results Included under Tab B of this Report are copies of all laboratory analytical results for thegroundwater quality samples collected under Part I.E.l of the Permit for the euarter,aiong with the laboratory analytical results for the fieid biank (MW-60) and the duplicate sample for MW-l1 (MW-63). 2.3.2. Analysis of Laboratory Results Under the Permit it is intended that background groundwater quality will be determinedon a well-by-well basis, as defined by the mean plus second standard deviationconcentration. The Mill is currently in the process of working with the Utah Division ofRadiation Control to establish background (including the mean plus standard deviation)for all of the constituents being sampled under the Permit. Until such time as backgroundis established, however, the Permit requires that constituent concentrations in eachmonitoring well shall not exceed the Groundwater Compiiance Limits (,,GWCLs,,) setout in Table2 of the Permit. Review of the analyical results indicates that concentrations of the following constituentsin the following monitoring wells exceeded their respective GWCLs in Table 2 of the Permit: Monitoring Well and Constituent GWCL frell) Sample Result (rnp/l\ Iron 2,750 3.190 Lead 3.75 29 ilaW-t+ fCtass ttt=Water) Manganese 400 1,860 Uranium 15 6s.1 ViW-20 (Ctass Itt WaO Manganese Uranium 400 1,350 15 22.4 Chloroform 3s 230 I t t I I I I t t t I I I T It should be noted that the anomalously high iron concentrations in some of these neutralpH groundwater samples suggests that the high concentrations of metals that were detected in these samples resulted from high suspended solids in the samples. MilIpersonnel have been advised of this and the need to pay particular attention to proper filtration of water samples in the future. Notice of these exceedance s was given to the Executive Secretary on June 10, 2005, pursuant to Part I.G.1.a) of the Permit. Pursuant to Part I.G.1.b)1) of the Permit, the Millwill commence accelerated sampling of each of the foregoing constituents in itsrespective well on a monthly basis, commencing in June 2005. 2.4.Depth ro Groundwater Readings And water Table Contour Map A listing of groundwater level readings for the Quarter (shown as depth to groundwater infeet) is included under Tab C. Also included under Tab C is a water table contour map, which provides the location andidentity of all of the wells andpiezometers listed in items 2.1.(b) above forwhich depthto groundwater was taken during the Quarter, the groundwater elevation at each such well and piezometer, measured in feet above mean sea level, and isocontour lines to delineate groundwater flow directions observed during the Quarter's sampling event. The contourmap uses the March 2005 data for the wells and piezometers listed in Tab C. However,for the monitoring wells not sampled in the Quarter, the June 2005 depth to groundwater measurements were used, as those measurements were considered to be the most representative data that is available for those wells. Quality Assurance Evaluation And Data Validation Quality assurance evaluation and data validation procedures in effect at the time ofsampling were followed. These involve three basic types of evaluations: field eCchecks; Analyticai Laboratory checks; and checks performed by Mill personnel, as described below. Monitoring Well and Constituent GWCL ftrg/l) SampIe Result (pell) ItztW-:Z f Ctass ttt Water) Berylium 2.0 2.6 Cadmium 2.5 23.8 Iron 5,500 9,780 i,ead 7.5 16 Manganese 400 3,740 Nickel 50 71 (i) (ii) I I I I I I t I I I I I I I I I I 2.5.1. Field OC Checks The following QC samples were generated by Mill personnel and submitted to theAnalyical Laboratory, in order to assess the quality of dutu resulting from the fieldsampling program: a) One field blank (MW-60); andb) One duplicate sampie of MW-11 (MW-63). These samples were sent biind to the Analytical Laboratory for analysis for the sameparameters as the other field samples. 2.5.2. The Analyical Laboratory has provided a summary repoft of the analy,tical qualitycontrol/quality assurance (QAiQC) measurements necessary to maintain conformancewith NELAC certification and reporting protocol. The Analyical Laboratory eA/eCSummary Report, including copies of the Mill's Chain of Custody and analyticat Request Record forms, is included under Tab D. 2.5.3. Mill OA Manaqer Review The Mill QA Manager, which is the Mill's Radiation Safety Officer, performed threetypes of reviews: a determination of whether Mill sampling personnel followed Millsampling procedures; a review of the results from the Eieia qC Checks; and a review ofthe Analy'tical Laboratory QA/QC analysis. The results otttre QA Manager's review arediscussed below. a) Adherence to Mill Sampling SOps on a review of adherence by Mill personnel to the existing sampling Sops, the eAManager made the following observations: !u_e to unfamiliarity with the requirements of the permit, the Analy.ticalLaboratory was not requested to anaryze for the following pu.u*Lt"rr,carbonate, bicarbonate, sodium, potassium, magnesium, calcium, and totalanions and cations. Those analytes wir be included in all future analyses; !u9 to unfamiliarity with the requirements of the permit, the AnalyticalLaboratory was instructed to use the State Ground water euality Standards("GWQSs") as the minimum detection limits ("MDLs,,), iather than one-quarter of those standards, as required for the GWCLs for Class II groundwater.This resulted in four cases where the minimum detection limit exceeded theGwcL. All of these were for MW-lr, which was the only well sampled thathas class II groundwater. These are chromium, where th; GwcL is 25 mgfland the MDL is 50 mg/l; molybdenum, where the GWCL is 10 mg/l and the I T t T I MDL is 20 mgll; thallium, where the GWCL is 0.5 mg/l and the MDL is 1.0mg/l; and vanadium, where the GWCL is 15 mgil and the MDL is 20 mg4. Theanalyical results for all of those parameters in MW-11 were non-detect at thoseMDLs. The Analytical Laboratory has been instructed to use one-quarter of the GWQS values as the MDLs, commencing with the2nd quafter ru*pliog event; (iii) The QA Manager concluded, after discussions with IUSA's geochemical consultant, that the anomalously high iron concentrations in some of these neutral pH groundwater samples (i.e., 3,190 p,gll in MW-I1 and 9,7g0 ltgllinMW-32) suggests that the high concentrations of metals that were detected in the samples resulted from high suspended solids in the samples. Mill staff will pay particular attention to proper filtration of water samples in the future; and (iv) Mill personnel inadverlently failed to prepare an Equipment funsate Blank and a Trip Blank. Mill personnel have been instructed to prepare such blanks and send them to the Analyical Laboratory for analysis for all future groundwater sampling events. b) Results From.Field QC Checks A review of the results of both eA/ec samples (the field blank, MW-60, and the duplicate sample, MW-63) indicate agreement of each anal1.te in each well and that the contaminant concentrations are suffi ciently accurate. 4 Review of Analytical Laboratory etltgg Analysis The QA Manager reviewed the Analytical Laboratory's QA/QC Summary and made thefollowing conclusions ; (i) Check samples were analyzed for all methods used in analyzing the groundwater samples. These methods were: I I I I I I T I I t T I Parameter Method Chloride A4500-Cl B Fluoride A4500-F C N itrogen, Ammonia as N A45OO-NH3 G Nitrogen, Nitrate + Nitrite as N E353.2 Sulfate A4500-SO4 E TDS 42540 C V4qls (other than iron)8200.8 lron F.240.7 Radionuclides E900.1 VOCs sw8260B I I I I T t I I I I I I I I I I I I T (ii) The check sampies included at least the following: a method blank, a laboratory control spike, a matrix spike and a matrix spike rluplicate; There were no qualifiers reported in the eA/ec Summary Report for any of the check samples for any of the analytical methods. All qualifiers, if any, and the corresponding explanations in the summary report are reviewed by the eAManager; There were no qualifiers reported in the Laboratory Analytical Report, other than an indication that the Reporting Limit was increased due to sampie matrix interference in the case of sulfate in all weils sampled. However, because theamount reported was well in excess of the increased reporting limit in all samples, the fact that the reporting limit was increased for sulfate had nopractical impact on the analysis; and (iv) (v) A review of the surrogate spiked samples for each sample showed no qualifiers. 2.6. Electronic Data Files and Format IUSA has provided to the Executive Secretary for groundwater quality monitoring conducted an electronic copy ofall laboratory results Values (CSV). A copy of the transmittal e-mail during the quarter, in Comma Separated is included under Tab E. 3. DMT PERFORMANCE STANDARD MONITORING Measurements Taken During the euarter During the Quarler, the following DMT Monitoring was performed or addressed, asrequired under Part I.8.6 of the Permit: weekly tailings wastewater pool elevations for tailings cells 1 and 3; Weekly slimes drain water levels; Weekly wastewater level measurements in Robert,s pond; and Weekly feedstock storage area inspections. Weekly Tailings Waste Water PooI Elevation Monitoring Mill personnel monitored and recorded weekly the elevation of wastewater in TailingsCells I and 3 to ensure compliance with the maximum wastewater elevation criteriamandated by Condition 10.3 of the Mil1's Radioactive Materials License. Saidmeasurements were made from an elevation suryey. The resuits of such monitoring,reported as feet above mean sea tevet (fmsl), are included in Tab F. Condition 10.3 of the Mill's Radioactive Materials License provides that freeboard limitsfor Cells I and 3 shall be set in accordance with procedures that have been approved bythe U.S. Nuclear Regulatory commission. under those procedures: (i) (ii) (iii) (iv) I I t I I I t I I t I I I I I t I I T (i) The freeboard iimits are set as per the January 10, 1990 Drainage Report for Cell 1 at a liquid maximum elevation of 5,615.4 fmsl; and (ii) The freeboard limit for Cell 3 is determined annually using a formula set out in the procedure. For the year October 7,2004 through September 30, 2005, the freeboard limit for Cell 3 was calculated under this procedure at 5,601.6 fmsl. In addition, Part I.D.2 of the Permit provides that under no circumstances shall the freeboard of any tailings cell be less than three feet, as measured from the top of the flexible membrane liner ("FML"). The top of the FML in Cell I is at 5,61g.5 fmsl and the top of the FML in Cell 3 is at 5,608.5 fmsl. This means that the maximum wastewaterpool elevations in Cells I and 3 permitted under PartI.D.2 of the Permit are 5,615.5 and 5,605.5 fmsl, respectively. As indicated in the table below, the waste water pool elevations in Cells I and 3, as measured during the Quarler, did not exceed these regulatory standards: 3.3. Weekly Slimes Drain Water Level Monitoring Upon approval of the DMT Monitoring Plan required by Part I.H.13 of the Permit, Mill personnel will monitor and record weekly the depth to.wastewater in the slimes drain access pipe at Tailings Cell2 to determine maximum and minimum fluid head before and after a pumping cycle, respectively. These measurements were not taken during the Quarter, but will be taken upon approval of the DMT Monitoring Plan, which is currlntly under review by the Executive Secretary. Part I.E.6.b) of the Permit provides that this requirement shall apply to Cell 3 only upon initiation of tailings de-watering operations. As Tailings Cell 3 is currently an active tailings cell and de-watering operations have not commenced, no such measurements will be made in the slimes drain access pipe for Cell 3 in the foreseeable future. 3.4. Weekly Wastewater Leyel Monitoring: Roberts pond Mill personnel monitored and recorded weekly, commencing on March g, 2005, theeffective date of the Permit, the wastewater levels at Roberts Pond to determine compliance with the DMT operations standards in Part I.D.3. of the Permit. part I.D.3 of the Permit provides that the water level in Robert's Pond shall not exceed an elevation of 5,624.0 fmsl. The results of such monitoring, reported as feet above mean sea level(fmsl), are included in Tab G. Tailings Cell Maximum Wastewater Elevation Measured During the Quarter(fmsl) Maximum Wastewater Elevation Permitted Under License Condition 10.3 (fmsl) Maximum Wastewater Elevation Permitted Under PartI.D.2 of the Permit (fmsl) Cell 5,615.01 5,615.4 5,615.5 Cell3 5,601.31 5,601.6 5,605.5 I t I I t t I I I t The maximum wastewater elevation measured in Robert's pond during the quarter of5,618.80 fmsl did not exceed the maximum permitted elevation of 5.624.0 fmsl. 3.5. Weekly Feedstock Storage Area Inspection Weekly feedstock storage area inspections were performed by the Radiation SafetyDepartment, commencing on March 8, 2005, the effective date of the permit, to confirmthat the bulk feedstock materials are stored and maintained within the defined areadescribed in the Permit and that all alternate feedstock located outside the definedfeedstock atea ate maintained within water tight containers. The results of theseinspections are recorded on the Weekly Mill Inspection Forms, which are available at theMill for inspection. No variance in stored maierials from this requirement or leaking alternate feedstock drums or other containers were observed during the inspections. I T T I I J un-27-05 )-' I WhiG Mssa Mill - Standard Opemting Procedures Book Enrironmenrcl Protection Manual, Section 2'2. Appendix E From-lUC BLANDING Locadon- l?tr";ll _ _ pH Buffer7.0 7- SpecificConductance nzo v'MIIOS/cm Depth to W*er 44.7* Temperarure (avg) Blt 678 2ZZ4 ATT{9HMENT 1 FIELD DATA WORKSHEET FOR GROUND WATER T-re4 P.00li F-41 5 /-\ ' Dure: 0E/00 Revision: l Page 1"1 ol l'l Date/Samplet t t z- Name endin.6ials 3/Vof a' ..u:1 pH Buffer 4.0--3&-- Yrell Depth 13 ? ' -Casing Volume (V) 4" Well: 17'5:-.('653h) 3" Well:--(.367h) iH of Warer (avil '1' 'f| . I I t I T I I I I I I I I t I I I I T Ii --_l l. I I i I I I Time: lr, ( ConductivitY Z t ?! Conductiviry ird-i Time: tr f I* Conductiviry ? t|) Temperature f fi Pumping Rate Calculatiou FlowRate (Q), in gPm' 5/60 = Comrnenls Time: 1L o { Conducrivity 4 & # Time ro evacuale two casing volumes (2V) a.\= A-U T=2VIQ= * SlCopy oi Mill PmccdurcsBook lI-Environmcrtrl Proccdurus\2,2GmundWucMppcndix E Sccrion 2'2 POC Phn-doc I T t T t T I t I I I t I I Jun-27-05 1l;32am From-lUC BLAltlDINc ATTACHMENT I FIELD DATA WORKSIIEET FOR GROUND WATER T-ts4 P.006 F-415 {"'\' t Date:08/00 Revision: 2 Page Ia of lJ 4. ts 801 6t8 2224 pH Buffer 4.0 ( White Mesa Mill- Srurdard Operating Procedures Book EnvironmenHl Protecilon Manual. Section 2'2, Appendix E I Date/Samplet , t Name and iniials,. 'lfialof tt-+ - I I Locarion 4 pH Buffer 7.0-, l.o , Specifi c ConducmnceJZ?---:uMHOS/cm Deprh to \Vnxs1 /at(.fl- ConduclivitY (ae)-'3 d Ternperarure (avg) ,? '5 Well Depth r?.[' ?, '. Casing Volume (\O 4" Well :-JL?-('653h)- 3" rS/eII;----J.357h) iH of Water (avgl l"'J' Time: to<?Time: Io1rl Conductivity,)$f .72';1 t7l -l ! I ConductivitY P ; v'(Tempenrure . l I ..1 i I I ] I I III Time: ru,({ Conductiviry-1i?7 Time: tofb conductiviry 3/ f l-gvlruuvrI tLJ ps L"( -I I I l, I t rrrrp.**r" 17-L remPeranrre 77J Puf.npirr s Rate Caleulaliqr Elow Rate (Q), in gpm'Time to evacuate two casing volumes (2V) 5/60 =T=2VlQ= I.' S:\Copy of Mill Proccdures\Book ll-Environmcntnl PmcedurcsV.ZGroundWateMpFcndix E Sccdon 2J POC Pho'doc --r Jun-27-05 ll:32am From-lUC BLANDINC 801 EIB ?224 T-754 P.00i F-415 Dare: 0E/00 Revisi$n:2 Pagc l'1of l-t /", t. White }i,lcsa Mill - Standard Operating Procedures- n""r., -g."i.nmenlal Prorccrion Mrnual, Section 2'2' Appendix E ATIACHMENT 1 FIELD DATA WORKSIIEET FOR GROUND WATEB-t l l.t,t -i _l I bate/SamPlerffi;;ffiinarc zholar d pH Buffer 7.0 1 ,a- PH Buffer q'a- 'v'!- SpecificConducunce r7?o'n\tlHOS/cm Depth ro lVarer . ConductivitY (avg Zt r D Temperanrre (avg {t'O Well Deprh lzz- f - Casing Volume (\) 4" Well: " ('653h)- g" well: ('367h) iHofWater (av1) b3 I I I I t T t I T I T I I I t I t I I Time:Tirne: ConductivirY : Ternperamre- . - Conductiviry p Temperature ' ' I.'-.,1 Time: Temperaturq Pumlin e Bate Calculation Flow Rate (Q), in gPrn ConductivicY Temperaturo . . Time ro evacuase two casing volurnes (2V) I .i I i 1 I 5/60 =T =ZYIQ= SlCopy of lvlill Proccdurcs\Book Il-Environmcr|ut Proceduns\2.ZGroundWaleMppendix E Sccdon 2'2POC Plcn-doc I I I T I I I I t I I t T Jun"?7-05 I I :33am From-l UC BLAtrlDING P01 678 ZZZ4 1-7s4 P.008 F-415 Dare:08/00 Revision: 2 Page 14 of l* r-(' \.. Whir{, Mesa Mill - Sr:rridard Opcraring Proceduncs s";i-r ErritonmenBl protecrlon Manual' Secilon 2'2' Appendix E ( ATTACIIMqNT 1 FIELD DATA WORKSHEET FOR GROUND WATER Date/SamPler t -Locarion fir.;<z (7.r,-r(. r?) . N"*t"nainitials vfeaL'-6- pH Buffer 7-0 7-o Specifi c Conductanse--!:,32-uMlloS/cm Wetl Depth r7o' ' CasingVolume (V) 4" Well: 7 z'7 ('653h) 3" Well:----(.367h) fH of Water (avil 6'tf ConductivirY (avg) 3 P-b - Ternperarure (ave\ dL3-- Deprh to Water ?7. st Ti*"' ttt"{Time:GTD ConductivitY !, bb Con&tctivitY 7l{b '' rr.frTernPeranrre. J' l, T l, Time: 1'Lal Timq 6fZ conductivitY 3(7o -Coa&tctiity 3U t"*prr*o. .. f il Tempercwra f6'J PumEting Rate Calculsdon Time ro evacuats rwo casing volumes (2V) T=2VIQ = 7-7'7Flow Rate (Q), in gPm- s/60 = =----/-D. I I I -) {.i5Plvla',.r i I I S:\Copy of lvlill Prpcedurcs\8ock ll-Envioomcnnl Proccduresu2Groundwrlrr\APPctldix E Sccrion 2'2 POC Plnn'do< - i Jun-27-05 I II "*t I I ll:33am From-lUC BLA|IDING 801 618 2?24 l-ts4 P.009/056 F-415 Date;08/00 Revision: 2 Page l.l of l* '(' White Mesr Mill - Stuhd'ard Operlting Procedurcs Book: Environnental Prote"don Manual, Sccrion 2.2, Appendix E ( - ATTACHMENT 1 FIELD DATA WORKSHEET FOR GROUND WATER Date/SamPlet ^t ) ./ Locarion fAr^r 6d Nri. una in irio* T lzul'>1 A pH Buffer 7-0 pH Buffer4.0 Specific Conductance-ulvlHOS/cm Temperanrre (avg) Well Depth - Casing Volume (v) 4" Well:-('653h)- g" Well:-(367h) pH of Water (avg) Time: Conducti t-iTime: '-l I I "-l I,l 1 I l -'-1 I:-,1. II 1,l ''l Ir-l j I I'l ..,1 I t I I I I I I T I I T I T T I I t I Conductivity p Tem_oeraEtre . Time: Conductivity hrmpin$ R4te Cslculation FIow Rate (Q), in gpm. 5/60= Time: ConducrivitY. pH-=- Temperanrre Time to evacuate two casing volumes (2V) T= ZVIQ = Comrnenrs Tr 4{a,-b . L-J 1 l I I.,..] l jJ I i s-rcopy of lvtill proccdur!5\8ook l1_EnvironmcoBl Procadurss\2.2GroundWsreMPP(ndix E scction f.2 POC Phn,doc Jun-?I-05 1 I :33am From-lUC BLAltlDIN0 ggl 878 2224 1-ts4 P.810/056 F-415 Dute:0E/00 Revision: 3 Pagc l{ of l.l - 'i':". Whirc lvleso Mill - Stl;aard Operating Procedures Book rnvironmenBl Protecdon Manual, section 2'2' Appcndix E ATTACHMENT 1 FTELD DATA WOBKSHEET TOR GROUND WATER DatelSamPler I ncetion tuw G3 Name and tniilals Tlzol't -{ (- pH Buffer 4.Q_-: {I I,1 Specific Conductance-uMHoS/cm Depth to Water Conductivity (avg) Well Depth Casing Volume (V) 4" Well: !'653h)- 3" well: ('367h) irH of Warer (avg) I t I I I I I I I t I T I I I t I I T Time:Time: Conductivity Tempenrure ' ConducrivitY. p Temperarure . Time: Conducrivity. Pumping Rate Calcul4tion FIowRate (Q), in pm, 5/60 = =. Comrnenrs Time: Conductiviry pH. Ternperamre- Time to evacuarc rwo casing volumes (2V) T =?YlQ= l Ii Il Sl\Copy of Mill proccdures\Book I l-€nvirBomconl Procc.durcs\2.2GroundwcrcMpFcndir E Sccdon 2-2 PoC Phn-doc I I Jun-27-05 I l1:33am From-lUC BLAl|iDINC 801 618 2224 T-784 P.01t/056 F-415 II,IWT@ ENEPGYLABOEATOBLES,INC..2SgS Salt}eekHtgnwly(a260/)'PO. 1o.x32Q.' Ca1PcG ryY8269 TotlFree 868.235,$15 , 307., yr, ' Fax 307.234.1639 ' casper@enegytab cc W.enewao,ctm ' I I.r I I LABORATORY A}IAIYIICAL BEPORT Client Iutemarional Uranium (USA) Coqp Project: 1st Quaner POC SauPliog Lab ID: C05040027'00I Report Datez 04119t05 Collection Date: 03/30/05 12: l8 Date Receiveik 04101/05 Metrix AgueousCllcnt SamPIe ID: -. MWI I MCL/ RL QCLI I I t t Anslyees MAJOR IONS Chlorlde Fluoride Nitrogen, Ammonla as N Nltrogen, Nllrate+Nitrlle as N Sulfate PHYSIGAL PROPERTIES Solide, Total Dissolved TDS @ 180 C METALS.TOTAL Arsenic Beryltium Cadmlum Chromium Cobalt Coppor lmn Lead MantBnese Mercury Molybdenum Nickel Selenium Silver Thalllum Uranium Vanadium Anc RADIONUCLIDES . DISSOLVED Gross Alpha mlnus Rn & U VOLATILE ORGANIC COMPOUNDS Acetone Benze ne Carbon tehachlorlde Chloroform Chloromelhane Merhyl eihyt ketone Merhylene chlorlde Rerutt Units Method Analysis Date i BY t_1 l-i 33 mglL 0.5 mgtL 0,61 mglL ND mg/L 1080 mg/L '1880 mg/L ND U$IL ND uglL NO ug/L ND ug/'l- ND ug/L 17 uglL o19o ug/L ZS ug/L 83 ug/L ND ug/L ND ugll ND uglL ND ug/L ND ug/L ND ug/L 0.6 us/LND ug/L 12 ug/L pCi/L ug/L ug/L uglL ug/L ug/L ug/L ug/L A4500.Ct B A4500-F C A45OO-NH3 G E353.2 A4s00,so4 E A2s40 c E200.8 E200,8 E200.8 E200,8 8200.8 E200-8 E200,.7 E200.8 E200.8 E200.8 E200.9 E200,8 E200,8 E200.8 E200-8 E200.8 E200.6 E200.8 ES00.1 sw8260B sw8260B SW82608 SW6260B sw8260B sw8260B SW826OB O4lO4lO513;561Jal O4rc7t1515:45 I stb Q4n4N511;31 /Jal 04/05/05 11;04 I )al Ul04lA513:19 / jal a4B4lO511r't9 / sl AGn4lOS 19;51 / bws 04/06i0s 14:18/ bws O4l04nS 19:51 / bws AN94Di 19:51 / bws A4rc41O519:51 / bws 0410410519;51 / bws 04/06/05 18t32 I q O4lo4l05 19;51 / burs A410410519151 I bws O4lO4lOS '19:51 / bvw 04/08105 14118 / bws O4l04lOS 19:51 / bws O4t04tO613:51 / bws O4lO4lO51Si51 / b$€ 04/04105 19;51 / bws A4n4E519:51 / bws 04/04/05 19:51 / bws 0!10410519;51 / bws 04/05/05 11:45 / rs 04/06/05 15:25 I rh 04/06/05 15;25 / rh 04/06/05 15:25 / rh 04/06/05 15;25 / rh 04/06105 15:251 rh 04/06/05 15128 I tn 04/06/05 15:25 / rh 1 0_1 0.05 0-1 30 10 5 0,5 0.5 50 10 10' 30 1 10 0.5 20 20 4 10 1 0-3 20 10 1.0 20 1.0 1.0 1.0 1.0 ZO 1.0 I I ND ND ND ND ND ND ND ND t t1 Report Detinitions; RL. AnalyIE reporting llmlt, QCL - Quality @nrrol limit, D - RL lncreased due to sample marrlx Interfercnce, MCL - Maxlmum contamlnant level- ND - Not detected at the reportlng llmil Jun-27-05I ll r33am From-lUC BLANDINc 801 618 2Z?4 T-is4 P.0l?/058 F-415 ENEBGY L/lBOfrAToRtEg tNc. , 23eA flaft Creek llrbhway (B26vt) ' P.O. Bat 92iP ' Caspcr; WY62802 ToltFree888.235.05l5 ' 3072 ...yrt ' Fax 3072,34-1639 ' casper@eneryylab.cx .,W.sneryytaa,com l-, I I I lr LABORATORY AI{ALYTICAL REPORT Client: International Uranium (USA) Corp ProJecE lst QuarterPOC SamPling Lab ID: C0504A027'001 ClientSampleID: MWll ReportDate: 04119105 Colleetion Date: 03/30/05 12;18 Date Received:. 04101/05 Matrix: Aqucous Analysis Dete /By MCL/ Qual RL QCL MethodResdt UnitsAn*lyses SWE26OB sw8260B sw8260s sw8260B sw8z60B SWBz60B SWE26OB SW8260B ND ND ND ND 100 96.0 86.0 101 "t I I I t T I ,-l 1 VOUnLE ORGANIC GOMPOUNDS ' Naphrhalene Tetrahydrofuran Toluene Xylenes, Total Surr: 1,2-Dichlorobenzened4 Surn Dibfomolluoromethane Sun: p-Brumofi uorobenzene Sur: Toluened8 ug/L uglL ug/L uS/L %REG %REC %REC %REC 1.0 1.0 1_0 '1.0 E0-120 . 70-125 80-120 80.120 o0o?os15*5/ rh 04/06/05 15:25 I rh 04/06/05 15;25 I rh 04/06/05 15i?S I rh 04/06/05 15!25 I th 04/06/05 1525 lth 04/06/05 15225 I rh 04/08/05 13t25 I rh Ii Ii l; -.i I I I t Rcpon RL - Analyte reporting llmlt.i Deficirions: eGL - euality conuol llmlr, ..t MCL- Maximum conEminant level, ND - Not detected at lhe rsporting limit. T I-, l-r Jun-Z7-05 I I :33am From-lUC BLA}IDINC s01 618 2?24 T-is4 P.0l 31056 F-41 5 sgwBw ENEFiY LABORATP4EA tMp. - frss Sat Crcel Highwy (sp6at) ' Po- ao.x szi7 ' Caspea ryf BZ00- To// Frae 888.235.05/5 ' 307.2 ylF ' Fax 307234.7639 ' casper@eneryytab-co .Yvt$.sneryyaD'@mI I l-i-l LABORATOBY ANALYTIC.AL REPORT Internadonal Uraniurn (US4 Cory Project: lst Quarter POC SamPling Lab ID: C05040027'00? Cticnt SamPleID: MW14 Report Date; 04ll9l05 Collection Date: 03/30/05 l0:57 Date Recelved: 04/01/05 Matrix: Aqueous .Aualyses Result Units Qual ]il'ICLI RI- QCL Method Analyeis Date / BYI t I T Fluodde-i Nlt.g*n, Ammonia as N , j Ntrogen, Nitate+Nldte as N Sulfale i PnYSICAU PRDPERTIESi solids, Total Dissolved TDS @ 1s0 c i METALS-TorAL Berylllum I ls#n Gopper I -l [iii""."" Mercury I.,Ui:iii#" Silver - i ThalliumI j vnxr,, ', Zinc t' *r,oNUcLtDEs'DtssoLVED Gross Alpha rnlnus Rn & U I I J n;1:*e oRGANrc coMPouNDs -. Benzeno r i ffr,.TffchrorideI chloromethano, MethYl ethyl keton€ I I Methylene chloride l,n-"- *" 'Chlorlde 21 rng/L0.2 rng/L 0.21 rng/L ND mg/L 2100 mg/L A4500-ct B AI500-F c A45OO-NH3 G E353.2 A450S,SO4 E AZE40 C E200.6 E200.8 E200.8 E200.6 E200"8 E.aa.8 E200.7 E200.E E200.8 E200.8 E200.8 8200.8 E200.8 E200-8 E2o0,8 E200,6 E200.8 E200.8 E900-1 swEZE0B SWB26OB SWE26OB SWEz60B SW8260B SWB26OE SWB26OB g4$at05't3159 / jal D41OTlOS 15;48 / slb 04/04/0s 11:33 /Jal 04/05/05 11:06/jal 04104105 13:20 /llal g4lo4n5 11r19 / sl 0uO4lA5 21;48 / bws 04/06105 15:16 / bws 04lO4tO521t4B I bvts 04n4fi5 21:48 / bws Oll14l05 21;48 / btats 04/04/05 21;46 / bws 04/96/05 1B:35/op 04104105 21i48 I buts 04l,04105 21;48 / bws 04104105 21:46 / bws 04/06/05 15:16/bvrc 04/04/05 21:48/ bll'/s 04104to521:48 I bwa 04/04i05 21i48 / bttrs 04104105 21:481bws 04/04/05 21:48 / bws A4lMl05 21:46 / bws 04n4n' 21;46 / bws 0410510511:45 / rs 0#08/05 16:11 / rh 04/06/05'16:11/rh 04/08/05 16;11 /rh 04/06/05 16;11 / rn 04/06/05 16:11 /rh 04/06/05 16|11 I rh 04/06/0516:11 /rh 1 0.1 0,05 0-1 30 10 5 0.5 0.5 50 10 10 30 1 10 0.5' 20 20 5 10 1 0.3 20 10 1.0 20 1,0 1.O 1.0 1.0 20 1.0 ND ug/L . ND ug/L'1,2 udL ND ug/L ND ug/L ND uE/L 83 ug/L 1 uAlL 1680 ugtL ND uglLND ug/L 24 ug/LND ug/L ND ug/L ND ug/L 65.1 ug/L ND uglL 17 uslL 3510 mg/L ND pCi/L ND ug/L ND ug/L. ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L Rcpon RL - Anelyre rePorting llmll Delinitiono: OCL. Quality conlrol llmlt- D - RL IncreEsed due to samPle matrix Interferance, MCL - Marlmurn con6mlnant level, ND - Nol debqied at lhe reporting limir Jun-Zi-05 1 I r33am From-lUC BLANDING 801 678 2224 I-7s4 P.0t4l056 F-415 ENEEGYL/IBORATUfrnES,WC-.zsgsSaltcreekHighwiiy(82601)'P.o.Eox3Q5Q'.CasW|WY82603 Totl fiee 888.235.05/5 - 30ZI yrt , Fax 3078.4-1639 ' casper@energylab.c( Yww.anewaD.dtnt I I I LABORATORY ANALYTICAL REPORT I i Cli"nt; Intemarional Uranium (USA) Corp ProjecL lst Quaner POC SamPling '-.1 lab ro: cl5o4oo27-oo2 Client SarnPleID: MWl4 ReportDatez 041t9105 Collection Date: 03/30/05 l0:57 Date Received: 04/01/05 Matrin Aqueous tvlcLl I-t ! Ij ll IIli Analyscs VOLANLE ORGANIC COMPOUNDS NaphihalenE Tetruhydftruran Toluene Xylenes, Total Sun: 1,Z-Didtlorobenzened4 Surr tribromofl uoromehana Surr: p-Bromofl uorobenzene Sun: Toluene-d8 Result Unih Qual RL QCL Meuhod ND .ND ND ND 100 s0.0 92,4 102 uglL ug/L uglL vglL %REC %REC %REC %REC 1.0 1,0 1.0 1.0 80-120 7E-125 80-1 20 60-120 SWB26OB sw8250B SWEZ6OB SW826OB sw8260B sw8260B SWB26OB sw82608 Date / By 04/06/05'16r'll /rh 04/06/05 16:11 /rh 04/06/05 '16:11 / rh 04/08/05 '16:11 / rh 0410610516;11 / rh 04/06/05 16;11 /rh 04106105 16.11 I th M/06/05 16:1'1 / rhI I ll tl li ll lr I"l I It'Repon RL - Analyte reponlng llmil Definltlonsl eCL - aua[rty conrol llmit. MCL - Maximum contamlnant level, ND . Not det€cted a[ the reporting limlt. Ili t Jun-27-05 I1:34am From-IUCBLANDING 801 678 2224 t-7s4 P.015/056 F-415 ENEfrGyLABofrATORtEg WC. , zaes buttcreekHlghway(82601)'Eo. Boxsffi ' Caspel W82602 ro//fiee888.235.0515 - 307.1 YrU ' Fx307,234-1639 ' caspel@enetilab.ct ',ywvr'enatgytso.comI I I LABORATORY ANALYTIC.A.L REPORT Client Inremational Uranium (USA) Corp Project: 1st QuarterPOC SamPling Lab ID: CA5O40A27'003 ClientSarnPletrD: MW26 Report Datc: Q4119105 Collection Dste; 03/30/05 I 0:1 5 Dgte Reeeive* 04/011A5 Ulatrix: Aqueoustr Analyses Rrxult Uuits Qual TVTCLI RL QCL Method Analysis Date /Byt I; Ij 1 0,1 0,05 0.1D30 10 5 0.5 0_5 50 10 10 30 1 10 0.5 20 2A 5 10 t 0-3 20 10 mglL mg/L mg/L mg/L mglLI'i l'i ll Ii 1.0 50 2.5 Z,J DE 2.5 50 pci/L poilL Ij I Iirl i I I I I T I MA^IOR IONS Chloride Fluorido Niuooen, Ammonla as N Ittrogsn, NifaE+Nllrlie as N SulEte PHYSICAL PROPERTIES Solids. Toral Dlssolved TDS @ 180 C METALS.TOTAL Arsenic Beryllium Cadmlum Chromium Cobalt Copper lron Leed Manganese Mercury Molybdenum Ntckel Selenium Silver Thalllum Uranium Vanadlum Zlnc RADIONUCLIDES - DISSOLVED Gnoss Alpha minus Rn & U Gross Alpha mlnus Rn & U Preclsion (t) VOLATILE ORGANIC COMPOUNDS Acetone Benz€n€ Garbon terachlorlde Chloroform Chloromethane Methyl ethyl ketone 3'110 mg/L ND ug/L ND rglL ND ug/L ND ug/L NB ug/L'ND us/L537 ug/L ND UdL 1350 ug/L ND ug/LND ug/L 25 ug/L I ug/LND ug/L ND ug/L 22-+ ug/L ND ug/L ND uglL 4.5 1.2 ND ug/L ND ug/LND ug/L 23O ug/L ND ual|- ND ug/L A4500-cl B M500.F C A45OO-NH3 G E353-2 A4s00-so4 E 42540 C E200-8 F2:00,8 E200-8 8200-8 E200.8 E200.8 E200"7 F,:00-8 E200.8 E200.8 E2OO,E E200.6 E200.6 E200-8 E200,8 E200.6 E200-8 E200,8 E900,1 E900.1 SW82608 SWB2608 SW82EOE sw8260B SWB26OB SW82608 O4l04lO5 14;03 / jal 0410710515:52 / slb 04/04/0s 11:35 / Ial 04/05/O5 11;09 / jal o4n4n51.3:?2llal 04l04NS 11;20 lsl t)4104/OS 21:56 / bws 04/06/05 15:23 / bw6 04/04/05 21:56 / bws 04t04tos 21:56 / bws O4lO4lO521:56 lb:t''r O4lO4l05 21:56 / bu6 04/08/05 18:38 / cp 0+104105 21156 / bws 04/04/05 21:56 / bws 0110410521i56 ltui 04/06/05 15;23 / bws MlO4/05 21;50 / btttrs 04/0{05 21:58 / bws 04/04/05 2'1:56 / buls 04/04/05 21;56 lbutt 04/04/05 21 156 / b\ Is 04i04/05 21 156 / bws 04/04/05 21;56 / bws 04/05/05 '1 1:45 / rs 04/05/05 11:45 / rs 04106105 20:00 / rh 04/08m5 20:00 / rh 04/08rc5 20:00 / rh 04/06/05 20100 I rh 0+/06/05 20;00 / rh 04/06/05 20:00 / rh 52 0.9 0-4s 02 18S0 D D D D D D Rcport RL - Analyte reporhng llmh Definltlons: eCL - euality control llmtl D - RL increesed due to sample malrlx lnlerferenoe, MCL - Maxlmum conbminant leval- ND - Not detecled at the reporting llmii.I' T-, I ll;34am From-lUC BLANDIllG s01 6ls 22?4 T-i84 P.016/056 F-415 ENERGY LABORATORTES, .IA{G . 2353 b-afi CE1K Hphway (B26tU ' nA Box 9250,' Casper; ry92y2 Tolt free 888.235.0515 ' 3022 yrg ' Fax 30229-16.?9 ' casper@enepylab.co ywwenetgyaa'comI I -.i .i LABORATORV ANALYTICAL REPORT Client: Intemadonal Uranium (USA) Corp Project: Ist Qua#erPOC SamPliug Lsb ID; C05040027'003 ClientSarnpleID: MW26 I t Report Dztel 04119105 Collecdon Dztet 03130105 10:15 Date Received: 04/01/05 Matrix: Aqueous MCL/ QCLI-i I l; T Il,lI ND ND ND ND ND . 106 95.6 92.0 107 ug/L ug/L ug/L ug/L ug/L o/oREC %REC %REC 6/oREC VOLATILE ORGANIG COMPOUNDS Methylene cnlorlde Naphthalene Tetrahydrofuran Toluens )iylenes, ToEl Sun: 1,2-Dlchlorobenzened4 Sun: Dibromofl uoromethane Surc p-Bromofluorpbenzeng Surn Toluene{B D D D D D D D D D 2,5 2.5 2,5 2.5 z-3 sw8260B. sw8260B SW826OB SWB26t)B SWEz608 80.120 SW6260B 70-125 sw8280B 80-120 sw8260B 80-120 SWB260B 04/06/05 20100 / th 04/06/05 20:00 / rh 04106/05 20:00 / rh 04/06/05 20;00 / rh 04106/05 20100 / fi 04/06/05 20:00 / rh 04/08/05 20:00 / Ih 04/06/05 20:00 / rh 04/06/05 20;08 / th lj li Ir li Ii t I Repon RL-Analyb raporting limit. DcGnitions: aOL - euallty conkol limit. D . RL increased due to sampla matrix interference, MCL - Maxlmum oonbminEnt level. ND - Not detected st the raporting llmlt,I t t Jun-27-05 ll r34am From-lUC BLANDING 9sl 678 2ZZ4 1-7s4 P.017/056 F-415 ri@IW ENEBGyLABoRArontEs.r'(c:.zrs! sa[e/eetrffl!-:rr[#Sig;,i;8 triffft;,_f,f;#frffifrr;'TiiiFree a8s255,0515 ' 307.2 . y15 ' Fax 307.234-16,19 ' casper@eneryyaD' tt t-, "j LABORATORY ANALYTICAL REPORT Clientr Inremarional Urauium (USA) Corp Project: 1st QuarterPOC SamPling Lab ID: CO5040021-0A4 Client Sample IDr MW32 Report D*ter Collecrion Drte: Dste Received: Matrir: a4/w105 03/30/05 13:14 04/0y05 Aqucoos t l Analyees Result Units Qual }IICLI RL QCL lVlethod Analysls Dete / Byt-i 1 MAJORIONS Chloride FluorideI T I t ', ttitroOen, Ammonla as N , _l Nirrogen, Niraie+NitritJe aa N -, tu'ot' * mg/L 0.2 mglL O,SZ rngll ND mg/L 2320 mg/L 3570 mg/L ND ug/L 2.6 ug/L23.8 uglL ND ug/L 37 ugA 51 uglL 9780 uglL 16 ug/L 374a ug/LND ug/L' ND ug/L 71 ug/LND ug/L ND uglL ND ug/L 4,1 ug/L ND uglL 594 ug/L M500-clB A450GF C A45OO.NH3 G E353,2 A4500-SO4 E A2540 C E200.8 E200,8 EzOO,E E200.8 E200-8 E200,8 E,20,0.7 E200.8 EzOD,8 E200..a E20A,8 E200.8 E200.6 E200_B E200,8 E200.8 EzOO,E E200-8 ES00.1 E900.1 swE260B SW628OB SWB26OB SW82608 SWB26OB SW82608 04nA10514:16 ljat 04107105'15:59 / Elh a4n4n511:37lial 04/05/05 11:11 /lal 04/04/05 13:24 I Jal O4N4IO5 11:20 I sl 04104t05 ?2;03 I bws 04/06/05 15:31 I bua 04IA4joS 22:03 / bws 04n4rc5 22:03 / bws O4l04lO5?20X I bv'ts 01.104105 22:03 I b\eg 04/08105 18:41 I cp 04l04lOS 22;03 / bws 04104105 22:03 I Dws. 04104105 22:03 / brvs 04/08105 15131 / bws OA|O4|OS 22:03 / bws 04l04lOS Z:03/ bws 0An4n5?2i03 lbr*s Ml04lO5 22;03 / bt*s 04104105 22:03 / bws 04104105 22;03 / bws 04104/05 22:03 I bws 04/05/05 11;45/rs 04/05/05 11:45/ rs 04/06i05 "10:57 / rh 04/06/05 16157 I rh 04/06/05 16;57 / rh 04/06i05 16;57 / rh 04/06/05 16;57 / rh 04/06/05 16:57 I rh 1 0-l 0.05 0-1 . 30 10 5 0.5 0.5 50 10 10 30 1 10 0.5 20 20 10 1 0.3 20 10. 1.0 li I.l lj PHYSICAL PROPERTIES Solids, Tohl Diesolved TDS @ 180 C METALS.TOTAL Arsenlc Berylllum Cadmium Chromium Cobalt Copper Iron Lead ManganesE M€rcury Molybdenum Nlckel Selenium Sllver Tha,lium Uranium Vanadium ztnc t T I I RADIONUCLIDES . DISSOLVED Gross Atpha mlnus Rn & U Gross Npha mlnus Rn & U Preclsion (t) VOLATILE ORGANIC COMPOUNDS Acelone Benzen€ Carbon tetrachlorlde Chlorofprm Chloromelhane Methyl ethyl ketone 2.4 pCilL 1,0 pcliL 20 1-0 1.0 1.0 1,0 20 ND ug/L ND ug/L ND ug/LND ug/L ND ug/LND ug/L Rcport RL - Analyte rgporting limit.Dclinition:: eCL- euallry contrcl limil MCL - Maximum contaminant level. ND - Not detecbd ot tha reportlng llmlt.lr il'' D - RL lncreased due to sEmple malrlx lnterference. I iun-Zi-O5 ll:34am From-lUC BLAl\lDING 801 678 2224 rte4 P.018/056 F-415r@EilF1f{r#f,?E{%fi|.;T ;',:'f,f'!t95;[r#!.:tfi"i&i,f;E:,tritr*'v,,fi1iffi'ffi.Yii' I t lt li .. 1 ll lr l_J l.i l,i li 'Ill IIl LAB ORATORY ANALYtr'ICAL REPORT Client Intemariornl Uranium (USA) Corp Project: 1st QuanerPoC SamPling Lsb ID: C0s040027-004 Client SsmPIe ID: MW32 S.eport Date; Collection Date: Drte Received: Matrix: 041t9105 03130/0513;14 04l0lt0s Aqueous MCL/ AnglvsesResultUnttsaryIRLQCLMethodAnalysisDgte/By VOLATILE ORGANIG COMPOUNDS MethYlene chloride Naphfialene T€trahydrsfuran Toluene Xylenas. Total Sun: 1,Z-Dichlorobenzened4 Su rc Dlbromofl uoromethane Sun: p-Bromgfluorobenzene Sun; Toluene'd8 ND ND ND ND ND 101 83-6 84-0 100 ug/L r:g/L rglL ug/L ug/L %REC %REC %REC %REC 1.0 SWB26OB1-0 sw8260B1-0 sw6260B 1.0 sw8260B1.0 sw8260B 80-120 SW82B0B 70-125 sw8260B 80-120 swB260B 80-120 SWEZ60B 04/06/05 16:7 / rh 04/06/05 16t57 I th 04/08/05 16:57 / rh 04106/05 16257 I rh 04/06/05 16:57 I rh 04/06/0s 16:.E7 I fi 04/06/05 16:57 / rh 04106105 16;,57 I rh 04/!6/05 16:57 / rh I I I I l ,,-,1 I i, Repon RL - Analyi€ reporting limit' DclinitiDnii eCL - Qualliy contrcl llmlt. MCL- Marlmum conErninunt level- ND - Not deteobd et the reponing llmilI T t Jun-27-05 I 1 r34attt From-lUC BLANDIN0 801 878 Z?24 T-ts4 P.0lsl056 F-415 ENERcy LAB-oqAroFtEs, r!c- ' z3eo satt ,*,0 ,H!-:v#;!3;:rhy11iff*ff;f:!rl{u1iT'riiiFiiiaas.iis.oiti . soz,i' lrc , rax 302234.161e - casper@enersytab.I l-LAE O RATORY ANALYI ICAL PSPORT I I Client: Internationel Uranir:m (USA) Corp Project lst Quarter POC SamPling Lab ID: C05040027'005 Client SumPle ID: MW60 Report Date: 041L9105 Collcction Date: 03/30/05 09:30 Date Received: 04/01/05 Matrix; Aqueous Analyses Recult Units QuaI twcLl RL QCL Method Analysis Date / BY 5 8.5 0.5 50 ,10 10 30 1 't0 0.5 20 20 5 10 1 0.3 20 10 I I I I t I I T I "i METALS-TOTAL I Arsenlc' .' B"ryllirrn Cadmlum ] chrornium -j coualt ftPPBr. lrcn f Laad .- ' Manganese Mercury 1 Molybdenum i Nictrel'" Selenlum Silver I rnattium i Unnium'-'' Vanadlum Zlnc ND ug/L ND ug/l ND ug/L ND ug/LND ug/L ND ug/L 3{ ug/L ND ug/L ND ug/LND uglL ND ug/L ND ug/L ND uglL ND ug/L ND ug/L ND ug/L ND ug/L ND uglL A4500'CtB A4500.F C A45OO-NH3 G E353,2 A4500-so4 E A2540 c 8200.8 E200,8 E200.8 E200,8 E200.8 E200.8 E?00,7 E200.E E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200,8 E900.1 SWBz608 SWB26OB SWB26OB sw8260B sw6260B SWE260B SWB26OB A4nU05 14i21 liat 0410710515:03 / slb 0410410511:39 / jal 04/05/05 11:14 I lal 04/U4/05 13:27 llal 04/05/05 15:10 / sl o4O4/05 22:10 / bws 04/06/05 15:36 / bws A4Eal0522:10 lbws o4to410522"10 lbM3 04/04/05 Z:10 / bws o4t04lo5?2110 I bvts 04/06/05 1B;45 / cp o4l04l15 22:10 I dtils 04/04/05 22:10 /bws 04/04i0522:10/bws 04/0e/05 15:38 / bws O4t041O522:10 I bws Oill4ni 22:10 / bws 0410410522210 lUvrs 04/04/05 Z:10 i bws A4l04tO5 22;10 I bws 0410410522:.14 I bws 04104105 22:10 / brlts O4l05lOS 11i45 t G 04/06/05 17i43 I th 04/06105 17t43 I rtt 04/06/05 17;43 I rh 0{/08/0s 17i43 I th o4lo6/oi fi:a3 lrh M/06/05 17!43 I th 04/06/05 t7:43 / rh MAIORIONS Ghloride Fluoride Nitrogen, Ammonia as N Nihogen, NItEte+NitriE as N Sufats PHYSICAL PROPERTIES Sqlids, Tobl Dissolved TDS @! 180 C ND.ND ND ND ND ND ND mg/L mg/L mgiL mgil- mg/L mg/L pci/L ug/L ugn- ugiL ug/L ug/L uglL trg/L 1 0,1 0.05 0,1 1 10 RADIONUCLIDES - DISSOLVED Gross Alpha minus Rn & U VOI.ATILE ORGANIC COMPOUNDS Aceione Benzene Carbon tehachloride Chloroform Chloromethane Methyl ethyl ketone Methylene ohloride ND ND ND ND ND ND ND 20 1,0 1.0 1_0 1,0 20 1.0 T I I I It Repon RL - Analyte reporting limil. Delinitionsr eCL - Quallty contol limit, MCL - Maximum contamlnant l8vel. ND - Notdetected at the r€ponlng limit. I . Jun-27-05 I 1 :34am From-lUC BLANDIllGL-.,801 EIB 2??4 T-794 P.020/056 F-415 t EitEnGY LABABATaRIES,.IA{C . 2393 Satt Graek il1glway (s260t) 'EO. Box 3ffi8.,' c81P?!_yY8-Y!2 Toll fiee 888.235,0515 . 307.2 .yr, ' Fax 307.2il.1639 ' caspsr@eneryylab,clc .Ytvw:energyaD.cvn l.r Il- LABORATORY ANALYfl CAI REPORT Client Intemational Uranium (USA) Corp Project: lst QuenerPOC SamPling Lab ID: C05040027'005 Ctienr Sample ID: MW6O Report Date= 04ll9lA5 Collection Dste: 03130105 09:30 Date Received: 04/01/05 Matrix; Aqueous I I Auslyses MCL/ Result Units Quql RI QCL Metbod AnalyslsDate/By ND .ND ND ND 104 o-t , 80.4 100 lt l.t lj I I I I I VOLATILE ORGANIC COMPOUNDS Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surn 1,2-Diclrlorobenzene{4 Surn Dibromofl uoromethans S um pBromofl uorobenzene Surr: Toluened8 vglL ualL ug/L u9a %REC ToREC %REC %REC 'l-0 1-0 1,0 1,0 80-120 70-125 BO-120 B0-120 04/06/05 17t43 I rh 04/06/05 17:431rh 04/06/05 V;a3lrh 04/08/05 17143 I th 04/06/05 17:43 / fi 04/06/05 17i43 I th 04/06/05 17;43 I ln 04/0805 17i43 t th sw8260B SW826OB sw82608 sw8260g swE260B sw8260B sw8260B SWB26OBlt ll ll il' I l.i Report RL - Analyh reponlng llmit,Ilcfinitions: eOL - euallty conbol limil MCL - Maximr-:rn contarninant level. ND - Not detecled at the raponlng llmit, I r-r J,n ilos_ I ll r35am From-lUC BLANDING g0l 6lg z?24 T-7S4 P.021/056 F-415rwENE^GY LAEOPATOBIES,.IUC. . 23e3 ,at Creek Hlghway (s2s0!l ' F.o. Box H50.. ' cespil ryY 8?0^' iliFiiiaaa-ia5q77; : 3f7j"-$to-:-fi sozzst.rcSe .'dsperdeneryytab.u ytwwenergvlab.com I I LABOI{ATORY ANALVTICAL R.EPORT r-lt-_lCfent: International Uranir:m (USA) Corp Projecl! lst QuanrrPOC SamPling 'iLetm: ca5o4oo27'oo6 , ri CEent SamPle ID; Mw63 Report Date: 041i9i05 Collccrion Date: 03/30/05 12:18 Dste fteceiverl: 04/01/05 Mstrixl Aqucous Result Units Qual RL Method A$alysit Date / BY MCTJ QCLIAnalyses MAJOR IONS --'Chloride I Arsenie Eerylllum Cadmium1 !Chromium Cobalt Copper lron Lead- rManganese MBrcury Molybdenum NIckel Selen;um Sih,er Thalllumi lnailrum I Uranium"' Vanadium Znc ND ND ND ND ND a) 3170 aa 89 ND ND ND ND ND ND 0.7 ND 10 I I I I I I t I Fluoride '"-l t{tr.og"n, Ammonia as N , I Nltrogen, Nlrate+Nitrile as N Sulfate ..| I rnystcnu PR0PERTIES' I solids, Total Dissolved TDs @ 180 c I METALS. TOTAL 1840 mg/L A4500"et B A4500.F C A45OO.NH3 G E353.2 A4500-so4 E A2540 C E200.8 E200.8 E200.8 E200.8 E200.8 E200-6 E20A-7 E200,8 E200.8 E200.8 E200.8 8200.8 E200,8 E200.8 E200_8 E200.8 E200.8 E200,8 E900.1 SW826OB SWE260B sw8260B SW8260B sw8260B sws260B sw8260B 04/!4/05 14;241 lal C/,li7l0516:07 / elb a4l04n5 Q;31 tial 04/05/05 11:24llal 04/04/05 13i28/jgl 04/M/05 11120 / sl oLlo4lA52:251bwE 01/06/05 15i45 / bvls 04rc4l15?2,;251bws 04/04/05 22;25lbvla 04/04/05 2225l buls 04n4n5 22:28I bvts 04106/05 1B:4Bl ap 04l04lOS 2Zt25 t bv,!g 04/04/05 2:?5 I bvts 04/04/05 ?2i251bv.ls 04/06/05 15:45 / bws 04/04/05 22:25lbuts 04/04/05 2:Z5l b\t'ts 041041052:25 lbws 03104/05 22:25 I bws 04lO4l05E;25 t bws A4N4l05 Z:25l bws 04n4n5n"?5 lbws 04/05/05 11:a5 / rs 04/00/05 18:29 / rh 04/08/05 18:29 lrh 04106/05 1829 / rh o4/o6/os 1E,129 I fi 04/06/05 18:29 / rh 04/06/05 16:29 I rh 04106/05 18;28 i rh 31 mglL 0.5 mg/L 0.80 mg/L ND mg/L '1180 .nalL ND ND ND ND ND ND ND I RADIONUCLIDES . DISSOLVED Gross Alpha mlnus Rn & U VOLATILE ORGANIC COMPOUNDS Acslone Benzone Carbon tekschlofide Chlorofunn Chloromelhane Methyl ethyl kebne Methylene chlorlde ugiL ug/L ug/L ug/L ug/L ug/L uglL ug/L ugll ug/L uElL ug/L uglL ug/L uglL ug/L ug/L ug/L PcilL ug/L ug/L ugiL uglL ug/L ug/L ug/L 10 5 0.5 0-5 50 10 10 30 1 10 0,5 20 ?o E 10 1 0.3 20 10 1.0 I I 20 '1.0 1.0 1.0 1.0 20 1.0 I Repon RL - AnalYte rePorting llmlr / nenntUons: eCL - euatity control limit. -- t D - RL lncreased due to sample matrix lnlerfarence. MCL - Maxlmum contamlnant level. ND - Not detectod at the reporting llmlt. I . Jun-Z7-05 l1:35am From-lUC BLANDING 9Et 6t8 ???4 T-ts4 P.0??/s5E #trf {,#f,?Ef{%ffi5;";'#![9tr]:iw":w8;:,3,tr;T;,,tr:i;'6'%tr;', F-41 5 I I l-l ] LABORATORY ANAL}MICAL REPORT Client: Iutcrnational Uranium (USA) Cory Frojecn lst Quarter FOC SamPling Lab ID: C05040A27-a06 Client SarnPIe [D: MW63 Report Date: Collection Date: Dete Received: Mqtrix: 04119105 03t30to5 a4toltD5 Aqueous l2:l8i I i Analysic Datp / BY NICLI Result Units Qud RL QCL MethodAnalyses ND ND ND ND 106 99.6 ts52 10'l lt li Il t VOLATILE ORGANIC COMPOUNDS Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun': 1,?-Dichlorobenzene-d4 Surf: Dibmmofluolomethane Sun: p-Bromofl uorobsnzene Sun: Toluened6 ug/L ug/L ug/L uga %REC o/oREC %REC %REC 1.0 t_0 1,0 1.0 E0'120 70-125 80-1?O B0'120 sw8260B sw8260B SWB26OB SW826OB sw8260B SWE2BOB SWA260B sw8260B I 04/06/0s 18;2\l rh 04/06/Ds 19i2q I fi 04/06/05 1&2q / rh 04/06/05 1&2Q / rh 04/06/05 18:2q / rh 04/08/05 18r2fl/rh 0410610318;2q / rh 04/05/05 18:29 / rh li Ir Ir I; li l.r Il I I Report RL - Analyle reporting llmlt. Dclinitiors: eCL - Ouallry control limil MCL - Maxlmum conbminant level. ND - Nol det€c1€d ar the reporting limlt. Il' : I'i t.a F6=a, nn27 Dah6 I - i Jun-28-05 06r48am From-lUC BLA}IDIN0 801 679 ?ZZ4 T-795 P.Bg\/ss?, F-4tg l I 'l I .t ii :--.1 Water Levei Readings for l.*t Quarter 2005 MWI L -94.37 MW14 - 104.31 IvIW2O -79.43 NNV22-70.20 MW26 - 70.2t (continuous pumping well) MW32 - 79.s8 Pt -70.74 P2-12.70 P3 -31.?6 P4 - 53.85 Ps - 46.68 Ivfvir4 -79.48 TW4-A -78,86 TV/4-1 -66.37 T\rr4-2-'74.63 TW4-3 - s1.88 TW4-4 - 68.90 TW4-5 - 55.72 TW4-6 -79.27 TW4-7 -74.41, TW4-8 -72.79 TW4-10 -57_42TW4-11- 69.78 TW4-t2-37.67 TW4-13 -69.28TW4-14- 90.91 TW4-16 -65.37 TW4-18 -56.26 TW4-19 - 80_21 I I l I t I J un-Z 7-0 5 I I :35am F rom- I UC BLAND I NG 801 Btl'2??4 1-754 P.023/056 F-41 5 ENEHGY I-ASOHATOP|ES, lNC. ' 23s3 Satt Oeek Ht1hwsy (s2601) ' P.O. po.x 32i0. - QsPr'; ff Ae0oz TollFree88s.235.0515 . 307.2 yt' ' Fax307.234.1ffi9 ' Hsper@enargylab-e1 .Wsneryyao.com I I I I I I I I I t I t I T I t I I I QA/QC Summary Report CIienI lilemarional Ureaium (USA) Colp Project: Ist QuartPr POC SamPling ReportDate: Work Order: 04lt9tos c05044027 Mothod: A2540C Sample lD: LCS1-050404A Sollds, Totiat Dlssolved TDS @ 180 C Sample lD: MBLKI;0504{!4A Sollds, Total Dlssolved TDS @ 180 C Samplo lD: C050t1{1027406CI'rS Solids, Toul Dissolved TDS @ 180 C Sample lD: C05040027-{I08CMSD Sollds. Total Dissolved TDS @i 180 C SamplelD: C05040081-00ZABUP Sollds. Tobl Dissolved TDS @ IE0 G Sample ID: C050rfi106:H)02AirS Solids, Tolat Dissolved TDS @ f 80 C Sample lD: Sollds, Total Dissolved TDS @ 180 C Sample lD: . LcSz-050404A Solids, Toral Dissslved TDS @ 180 e Laboratory Control Spike 896 mg/L Method Blank ' ND mg/L MahixSplke 11900 mg/L Matdx Spike Duplicate 12000 mglL Sample Dupllcate 15900 ffiAlL Matrix Spike 118000 mglL Mabix Spike Dupllcare 118000 rng/L Labomtory Conhol Splke S80 mglL 10 6 10 10 10 10 g0 04/04/05 11;18 04104105 11;18 0N04lA5 11i21 Otl}4lOS 11;?1 10 04/04/05 16:09 10 04/04/05 16:1 0 0UA4|O5 1e:10 10 04/04i05 15:10 101 s0 ra 101 90 110 0,4 10 10 102 g0 110 s.2 10 gE 90 110 110102 Result Units RL %REC Low Limlt Hlgh Llmlt RPD RPDLlrnlt Qual Batch : 050404A-SLDS-TDS-W QuaIlIIers: RL - Analyte reportlng limil.ND ' Not detected at the reponJng llmlt. 1 1 r35am From-lUC BLANDINC 801 678 ZZZ4 T-784 P.024/056 F-415 EtttERGy LABORATOqES,INC. ' 2993 6a/r Creek Hlghway (0260/) ' EO. Box s&4 ' Caspcc W 82602 Toll fiee 888235.0515 . 907.2' yl, . Fex 307.234.1635 , casper@energylab.co Wanergyw-con QA/QC Surnmary Report Client: Intcrnational Uranium (USA) Corp Project ist Quartcr POC SamPiing Report Date; 04119105 WorkOrdcr; C05040027 I I t I I I t I I I I I I I I t I T I l l Msthod: 42540 C Sampte lD: LCSI-050'105A Sollds. Total Dissolved TDS @ 180 C SamplelD: MBLK1-050405A Solids, Total Dissolved TDS @ 180 C Sample tD: C0504!1093-008AMS Solids, Total Dissolved TDS @ 180 C Sampla lD: C05040093-O08AMSD Sollds, Tqtal Dlssolved TDS @ 180 C Sample lD: C0504013440{CBUP Solids, Total Dlssolved TDS @ 180 C Sample ID: C05040134-00|CMS Sollds, ToEl Dissolved TBS @ 160 C Sample ID: G05040134-00tcMSD Solids, Tolal Dissolved TDS @ 180 C samplelD: LCS2_050405A Solids, Total Dissol\red TDS @ 180 C Laboratory Control Spike 996 mg/L Mehod Blank ND mS/L Matril Spike 26290 mg/L Makix Spike Duplicate 26300 mg/L Sample Duplicato . 2A1,A mg/L Mabix Spike 13100 mg/L Matrix Spike Dupllcate 13100 mg/L Laborarry Control Spike S79 mg/L Batch; 0504054-3 LDS"TDS-W 04105t0511tc.z 04/05/05 1 1:02 04/05/05 1 1;05 04105105 11:05 0.4 10 M/05/05 15:33 12 10 04/05/05 't 5:33 04/05/05 15:34 10 04105/05 15:34 99.6 1'1090 110 110 g0 90 ,o: 102 10 10 10 10 90 80 s097.S 10'l 10? Result Uniis RL %REC Low Limlt Hlgh Limit FPD RPDLimit Qual Method: M500-Cl B SamplolD: MBLK9-{150{O4A Chloride Sampla ID: C050.002?imC Chloride 9ample lD: G0504002?'003tr Chloride Sample lD: LGS35.O50404A Chloride Samplo lD, M8LK36.050404A Chloride Methoc, tslank ND mg/L MabixSpike 231 mg/L Matrix Spike Dupllcate 229 mg/L Laboratgry Conirol Spike 3500 mg/L Method Blank mg/L 110 110 s0 90 1.0 t-0 ,-0 101 ss.9 98,6 Baich : 058104A-CL-1TR-w O4l0l,lOS 12t29 o4rc4105 14t13 0410410514114 0.8 10 o4to/,tos 14;26 O4lO4lOS 14t26 :.] Qurliliersr RL - Rnalyte reporting limit. t_l ND - Not detecled at lhe reportlng limil. I I I I I I I I t I I t I T I I T I I Jun-27-05 llr3Sam From-lUC BLAI\{DING Bg1 618 2ZZ4 T-7S4 P.025/05S F-415 ,= ENEBGYLABaEATzflES,t$-c.-zSgssaltcreekHighway(d260t)'P.o.Eox1Z$Q'Casper,Ywaa602lE!ru TnrfiepBEEp3sn515,30z2' " \6/5, Fax30Z234-1639. casoer@sneruylab,cvr \vvweneqylab.com Ii ' QA/QC Sumnrary Report Client: Inremational Uranium (USA) Corp Report Dstaz 041ry/A5 Projectu lst QuzncrPOC Sampling Work Ordert C05040027 Analyte Result Unitrg RL %REC Low Llmlt Hlgh Limii RPD RPDLlmlt Qual -tI I i--l I Method: Sample lD: Fluoride Sampla lD: Fluonde SEmFle lD: Fluorlde Sample lD: Fluoride A4500.F C MBLKr-050407_1 c0503r{5540,IAMS c0503t155.{rHAlrrsD LCS1-050407_'l Method Blank ND mgA MarlxSpike 1,50 mg/L Matrix Splke Dupllcate 1-60 mg/L Laboratory Control Spike'1.10 mg/L 0_02 0.10 0,10 0.10 e5 90 1'10 105 90 110 110 s0 110 Batoh: 050407_1-F-lSE-W 04/07/051520 MlA7fiS 15:28 O4107105 15:32 5.s 10 04/07/05 16:36 -t Qualificrsl RL - Analyta r€ponlng Iimit,ND - Not detscled at rle reportlng llmit. I Jun-2i-05 1l;35am From-lUC BLAtlDIlrlG a01 ETs ??24 1-lg4 P 0?S/056Iir ffi ,ifF1f{,;irf&f;?i!82 5n'!'i,f![9trl flg!.:[!w&i,i,E ff ffqi,f,f:f:iitr tr;'..JTW F-41 5 i Client: ]uemarional Uranium (USA) Corp 1 P"olecu lsr Quaner POC SarPliug QA/QC Summary Report Report Date: 04/19/05 WorkOrdert C45040027 I t I I t I t I I I I I I I T T I ! I -t ,t.l Sample lD: G0503l05l.005BMSD Matix Spike Duplicate Method: A4500.NH3 G Sample lD: MBLK-'I Nitrogen, Ammonie ae N Sample tD: c0503{0s1.005BMs Nilrogen, Ammonla as N Nihogen, Ammonla as N Sample lD: MBLK.{7 Nltrogen, Ammonia as N Sample lD: C05031183.001AMS Nitrggon, Ammonis de N Nitrogen, Ammonla as N Sample lD: MBLK.32 Nibogen, Ammonla as N Sample lD: MBLK.48 Nitrogen, Atnmonla as N Sample lD: C0503,17E.1!03DMS Nitogen, Ammonla as N Sample lD: C05031178-003DMSD Nibogen, Ammonia as N Sample lD: MBLK{3 Nilrogen, Arnmonla as N Sample lD: G05M0028'004BMS Nltrogen, Ammonia as N Sample lD: G05040028-004BMSD Nlrogen, Ammonia ae N Sample lD: MBLK€O Nitrogen, Arnmonla as N Sample lD: C05031165-009AMS Nltrogen, Ammonia as N Method Blank 0.04 mglL Matrlx Spike 1,99 msll 2,11 mg/L Method Blank ND mg/L Marlx Spike1.ss ms/L 2.05 mg/a Meihod Elenk 0.04 mg/L Melhod Blank 0.03 mgll Matrix Splke' 1-92 rrlglL Matrix Spike Duplicato 1-BB mg/L Method Blank 0.04 mg/L Makix Spike 1.87 mg/L Matrix Spike Dupllcate 1.92 mg/L Method Blank ND rng/L Matrlr Splke 2,80 rng/L o"o2 0.050 s1 103 80 120 120 120 120 120 120 120 Batch: A2005-04{4-1 -NH3_01 04/O4l05 08:58 04/04/05 O9:1? 04/04/05 09:14 5.9 20 0d04l05 09:30 D4t9ot9aOgi4Z 04/04/05 O9;t14 5.0 20 M/04/05 10:40 o4to410511-.14 04la4l0s11:25 ul04l05 11._27 2.1 2A 0AtMl05 11:43 o1t0410511._87 04/04/05 1 1:59 20 0410il4512:,17 O4t0at0512;43 BO SamplolB, c05031163-{t0lAillsD MarixsplkoDuplicab 80 80 "_1 :i i 80 BO 0.o2 0-02 0.050 0.050 0-02 0.050 0-050 0,02 0.050 92.5 91.5 94 BO Result Unlrs RL yoREC Low Limlr Hlgh Llrnit RPD RPDLimit Qual Qurllfiersl RL - Analyte repoiling lirnit.ND - Not detected at the reporting limll Jun-27-05 I I :35am From-lUC BIAltlDIllG 801 6t8 2224 1-ts4 P.s?7/056 F-415I ENEBGY LABORAIOEIES, I\C, ' 2S9S Sa[i Creek Hrghway (5260U ' P.O, aox 33.-64\ ' CasPeG WY8260' T;tFEeABA.zg5.05t5 - s07I yru , Fax 307.2 ./63s . casper@energylab,ct _yww,eneryytaa.com QA/QC Summary Report Ctienfi hrternarional Uranium(USA) Corp. Project: lst QuarrerPOC SaurPling Report Dste: 04ll9lo5 lYorlr Order t C05040027 Result Units RL %REC Lowlimit HighLimit RPD RPDLimit Qual illerhod: M500-NH3 C Sample lD; C05031165.009A81SD Nltrogen, Ammonia as N Matrix Spilo Dupllcate 2.69 mg/L 0.050 80 Batch: A2005-04-04_1-NH3_01 44fi4105 12t45 120 3,? 20 I I I I I T I I t I t I I I I T I T I Method: Sampte lo: Sulfaie Sample tD: SulPale Samplo lD: Sulfate Sample lD; Sulfate Sarnple lD: Sulfale Ssmpl€ lDi SulhE Al'sogsotlE MBLK-1-050404 G0503,1143.00rAtlls c0s031,143{DtAMSD c0s040023-{r02BMSD LCS.I-050404 Batch; 050404-1-5 O+TURB-W Method Blank ND mg/L Matrix Spike 49.3 mS/L Marlr Splke Duplicete 4s.1 mg/L Marix Spike 35,1 mglL Matrix splks Duplicate 34.9 mg/L La bora tory Conlrol Splke 41.1 mg/L 110 110 0-4 @lO4lA5 12t40 o4lo4l05 1?:52 O+lOrrnS 12:-52 10 04104/05 13:17 04/04/05 13:18 10 04/04tII5 13;30 0-6 1.0 109 S0 1-0 108 90 1.0 102 90 1.O ''01 90 1.0 103 90 110 110 0.8 110,_l ",1 l Batch; 7600 u4l0d05 17:49 0d.10810517i52 Method: Samplo lB: Iron Sarnple lD: lron 8200.7 MBTBOB LCS,808 Method Blank 0,003 mglL Laboraory Control Spike 0.494 mg/L 0.003 0.030 98.7 11s85 QunllEerst RL - Analyte reponing llmlt.ND - Not qetectBd at&e reponing limit, Jun-2I-05t t 1 1 :35am F rom- I UC BLA}ID I NC .sil ETl ?2?4 T-784 P.028/056 F-415 ENEEGY |ABOEATORIES,.,4C. ' 2393 Satt Creek Hrshway (S1Wt) ' EO. Box 3154' Caspon WY 83602 h// Free 8d8.235.0515 , 30Zt fl5 ' Fax 30Z234-10i9 ' caspsr@ertergylab.ca -ywweneEyaD,con li I QA/QC Summary Report -, Cllenfi Inrernarional Uranium (USA) Corp j Projec* lst QuarterPoc SamPling Method Blenk 0.0002 rng/L ND mg/L ND mg/L o.ooo2 mg/L ND mSiL No ms/L . ND mg/L 0.0000S mSlL ND mg/L 0,0007 mgll ND mg/L 0.0008 mg/L 0.0002 ms/L ND mg/L ND mg/L ND mg/L 0,002 mg/L Laborall)ry Control Spike' Low 0-0180 mg/L 0,0134 mglL 0.0192 tltglL 0.0189 mg/L 0-0131 mglL 0.0130 ms/L 0.0191 mg/L 0-0192 mgA 0.0134 mglL 0.0188 mg/L 0.0953 ms/L 0.0192 mglL 0.0190 mg/L 0.0203 mgtL 0.0187 mg/L 0,0231 mglL Pre.Dlgestion Spike 0.0206 mg/L 0.0232 mg/L 0.0176 mglL 0"0455 mg/L 0.0002 0.00003 0.0002 0_0001 0,00003 0.0001 0.00002 0.00003 6.0E06 0,00007 0.00008 0.0004 0-00003 0.00003 0,00004 0-00009 0,0003 0:0010 88.6 0.010 97 0-010 96.1 0,050 83,20.010 s5.5 0.010 97.8 0.050 85.6 0.010 s5-80"10 93-4 0.050 s3.8 0_0010 s4.6 0_0'10 950-10 s5.2 0.00030 102 0.10 93.5 0.010 ,o: 0,0010 s1,8 0,010 1 16 0,010 88.1 0.050 96"e Report Date: 04/19/05 Wsrk Order: C05040027 M/04/05 15:37 O4fial05 15:44 l-r . "ilt Ii Ii Ir li lt li li li tl Method: E2oo-8 Sample lD: MB-760S Arssnlc Berylllum Cadmium Chromium Cobalt Gopper Lead Manganese Mercury Molybdenurn Nicxel Selenium Silver Thallium Uranlum Vanadiurn Zinc sample lD: LcSl-7608 Arsenlc Beryllium Cadmium Chrornlurn Cobalr Copper Lead Manganese Molybdenum Nickel Selenium Silver Thallium Uraniurn Vanadium Zina Sample lD: C050'10027-001DMSs Arsonlc Beryllium Cadmium Ghromium 80 BO BO 80 80 80 80 80 BO BO BO BO BO 80 80 80 70 7A 70 70 124 120 124 120 120 120 12:0 120 120 120 1Zg 1?A 120 120 120 1?o 130 't30 130 130 I I Resulr units RL 7"REC Low Lirnit High Limlt RPD RPDLimit Qual ND. Not detecled a! the reponlng limit. 04/04/05 1 9:59 I I Qurlificrs: RL - Analyte reporting limit. I I ENEBGY LAEO4ATOilES, lqc '23ga Salt Greek lltghwav (sfrOl)'EO- Box 3$Q ' Caspet tfry82602 Tol/Free888.235.05/5 , 307.2 yl, ' Fat 302234,1639 ' caspet@energylab.Co 'W-eneryytab,c0n Jun-2i-05 llr36an From-lUC BLANDING 8Bl 878 2224 T-is4 P.S?s/056 F-415)Efrru @ I t I QA/QC Summ2ly Report Clienfi Intenrarional Uranium (USA) Corp Projecr: lst Quartff POC SarPling Analyte Result unlrs RL "/oREC Low Limir High Llmlr RPD RPDLimit Qual Msthod: E2oo3 gatch:7608 I _, Sampto lO: CO5040A27{01DMS5 Pre-Dlgestion SPike 04/04J05 19;59 I I cobatt 0-0179 mgil 0-010 85 70 130' Copper 0,0348 rng/L 0-0'10 BB.4 7A 130 I Lead 0.0481 mg/L 0.050 96.1 70 130 f I Manganese 0.100 mg/L 0-010 70 130 Ar ; Mercuu 0.00847 mg/L 0-0010 M.6 70 130 Nickel 0,0334 mg/L 0,050 S9.7 70 130 I - Setenium 0.0986 mdL 0,0010 95.4 ?O 130 I i Thallium 0.01s7 ms/L 0.10 s8.1 70 130 Uranlum 0_0223 mg/L 0.00090 109 70 130 Vanadium 0-0222 mg/L 0.10 91.7 70 130I , ;;';'''"' ;:.;;;; ,il #;; "';u ;; ;;I I .Msrrixspikomctrvorl83OUrEldarheaccepbncocriledaofTOtot3Operc€nl,arEconsiderBdmalrixrslat6d,nottystemrol8led, RBporbdvaluEEBlBwilhinmolhod'rv,tsl[luPr^uruwvgl19]usErsq!rEEsPs,rwH(e'rsuUuru twPerl5rrrdEwu.,qErEUiltdulllutdlgurttul]]ElE[r,groEvr FtrPsrEs spscihcatione. (EPA Mathod 200,8, par, 9,d,4) Sampla lD: C05040027,001DMSD8 Pre-Digesdon Spike Dup 04/04/05 20106ll S8mplg llJ: r,U3U.IgU4r,UUluBlJuC rtF-LrrgEEusn DPltru UUP u+rr I i Arsenic 0.0208 rastL 0.0010 s?.6 70 130 0,7 20 - I Berylllum 0.0229 mg/L 0.010 114 70 130 1.3 20 Cadmium 0.0175 mg/L 0.010 86.8 70 130 1.4 ?O Report Date= 04ll9lA5 lVork Ordert C05040027 Chromlum 0.0424 mg/L 0.050 8't 70 130 o 20 Cobalt 0.0171 mS/L 0.010 81.3 70 130 4.3 20Copper 0.0827 mg/L 0.010 77.8 70 130 6.3 ZA Lead 0,0465 mdl 0-050 88-l 70 130 0 20 I I rrtrrgrnr.u 0,0986 rnStL 0-010 7a 130 1.4 20 A I i Mercury 0.00814 mG/L 0.0010 81"3 70 130 4-0 20 Nlckel 0,0336 mg/L 0.050 90.8 70 130 O 20 I I Selenlum 0.0881 mg/L 0.0010 95,8 70 130 0.8 20 I I rnutliu* 0.0187 mg/L 0.10 92.s 70 130 o 20I - Uranium 0.0215 mg/L 0,00030 105 70 130 3,6 20 Vanadium O,O207 mg/L 0.10 &.2 70 130 O 20 I I zin" 0.s246 mslL 0.010 62.8 70 130 1.8 20 S I ;$1il:"-,iJi::f#'i"frff8f:,"i1?:tfi, t*"P*nce critBria pr 70 lo 130 percent are considered marrix rersred, not syErBm ralated. Rcportod valuss are wlthlo method Sampla lD: MB.760E Arsenic Beryllium Cadmium Chromium Cobalt Copper Lead Manganese Mercury 04/06/05 13:56 I I :[:T',* Copper li t1 Ilr i l.l Method Blank ND ND 0.0002 0.0004 ND ND ND 0,00007 0,00003 mglL mg/L mg/L mg/L rng/L mg/L mgiL rng/L mg/L 0,0002 0.00003 0.0002 0.0001 0.00003 0.0001 0.00002 0.00003 6.0E-06 Qunlilicryl RL -Analyte reporting limil, ND - Not dateded at the reporilng llmlt. A - ThB enalyte level was greater than four llrnes the splke level, ln accordance wlth the method % reoovery is not cElcula!6d. S - Splke recovery oulside oI advisory llmlr- It' I 1 r36am From-lUC BLANDINC 8s1 67A ?U4 T-794 P.030/056 F-41 5 ENEEoYIAEORATOfrIES'"14C.'frgSSattareekHrsfiway{82601)'EO.gox9?5{'CasPcoWYSEEH To//Free888-235.0515 , 307.2 \f15 ' Fax 307-234./639 ' caspar@anegylab.co lwuanergylab.cont t ll Ir ) Q.A/QC Summary Report l.r Client: Iurernarional Uranium (USA) Corp Project: 1st Quaner POg $arurling Method: E200,8 Sample lD; ttlB-760s Report Date: 041L9/45 Work Ordcr; C05A4A027 04/06/05 14:04 04/06/05 14125 Method Blank 0,0002 mg/L ND mg/L ND m/L 0.0001 mg/L ND mdL ND mglL ND mg,fl 0.U02 mg/L Laboralory Control Spike --Lo!v 0.VZD1 ms/L 0.0177 mgn- 0.0209 mg/L 0.0211 mg/L o-O212 mglL 0.0200 mglL 0,0204 mg/L . O.O214 mg/L 0-4212 mg/L O,O2O1 mg/L 0.101 mS/L g.O2O7 mg/L A,O2Q5 mgtL 0.0200 mg/L 0-0206 rng/L 0.0231 mgrl Pre-Dlgestlon Spike 0.0216 mg/L 0.0163 mg/L 0.0183 mg/L 0.0477 mglL 0,0216 rng/L 0.9346 ms/L 0.05'|3 mg/t 0.120 mg/L 0.00939 ms/L 0-0240 mg/L 8.03U7 mg/L 0.0924 ms/L 0.0185 mg/L I I I I l- t1 I] lj i_l I I t I Molybdenum Nlckel Selenium Sllver Thallium Uranlum Vanadium Zinc Sample lD: LCS1-7806 Arsenic Beryllium Cadmlum Chromiurn CDbalI Copper Lead Manganese Molybdenum Niokel Salenlum Sllver ThEllium Uraniurn Vanadium Zina Sample lD: C05040027-0tl'lDMSs 0-00007 0-00008 0.0004 0.00003 0.00003 0.00004 0-00009 0,0003 0.0010 100 0.010 88.7 0.010 104 0-050 1010-010 1060-010 .100 0.050 1020.010 1050.10 1050,050 101 0.0010 101 0.010 1030.'10 103 0,00030 1000.10 1030-010 107 0.00'10 98_10-010 81 0.010 94.3 0.050 s7.2 0.010 1030,0I0 86,6 0.050 100 0.010 0,0010 93,5 0.10 105 0-050 a5 0.0010 91.3 0-010 91.4 Arsenlc Berylliurn Cadrnium ChrBmium Cobalt Copper Lead Manganese Mercury Molybdenum Nlckel Seleniurn Silver 8A 60 80 80 60 80 BO EO 80 BO EO EO 80 EO 80 BO 70 70 70 70 70 70 7A 70 70 70 70 70 70 120 120 120 1?.0 120 120 124 120 120 120 120 120 120 120 120 120 130 130 130 130 130 130 130 130 130 130 130 130 130 Resulr Units RL c/oREC Low Limit High Limit RPD RPDLimit Qual t Quuli{icrr; RL - Analfa reporting limit, ND - Not detecred at the reponlng limit- A - The analya level \ias greabr than four tlmes tha spke level' ln acmrdanoe with the method % recovery is not calculated- l't-* ih=6Aaaa7 Ooho I Jun-27-05 From-lUC BLAlllDItlG 801 618 2?24 T-is4 P.03t/056 F-415 ENERGYLABORATORIES,.UIG '2ssS6atCrcekHlghway(s2604'eO. 8oxS48-' Caspen vWB2502 Toll Free888.23505r5 ' 307.2 Y/5 ' Fil(307294.1639 ' caspar@energylab'co vtlfi4.eneryrylaa,com T I I I i J ---: Client: QA/QC Summary Report Inrcrnational Uranium (USA) CorP lst Quancr POC Sampiing Report Dste: 04/19/05 Work 0rdert C05040027 A 20 ?0 20 20 ai 20 20 20 70 20 2A zo 20 zo 70 7A 70 70 t I I t I I I T I I Ma?hod; 8200'8 Sample16; gg5grt0027{0lDM55 Pre-DigqstlonSpike 0,0210 mg/L 0.0163 mg/L 0.0.lB5 mglL 0,0457 mg/L A.O21O rng/L 0,0351 rng/L 0.0511 rng/L o-119 mg/L 0.00326 "rj.glL0,0239 rng/L 0.0309 rng/L 0.0901 rng/L a.OlTl rng/L 0.0208 mg/L O,O22O mg/L 0,0232 mglL 0.0251 rng/L 0-001D s4.8 0.010 80,80,010 92.7 0.050 92-1 0.010 99.80.010 89 0.050 99.2 0.010 0.0010 82.20.10 '104 0-050 860.0010 E90.010 87.20.10 103 0.00030 107 0-10 97.2 0.010 60.5 Batch 7608 Q4|AA05 14t25 04/06/05 14:33 20 2020s Thatllum Uranlum Vanadium Zino 0.0215 ms/L 0-0223 mg/L o.o237 ms/L 0.0265 mg/L 0.10 107 0.00030 108 0,10 s9-3 0.010 67-6 130 130 130 130 . Msbix Epit(e reco/eries outside he eccapbnce caiteria of 70 ro 130 percent are consldered matdx ralatod, no! Syslam related. Reportcd volue3 sr8 \,[lthin msthod apecificatJons. (EFA MBthod 200.8' par. 8.4.4) sampto lD: c05040027-00'tDMSDS Pre-Digestion Splke DuP Arsenlc Beryllium Csdmium Chromium gobalt Coppar Lead Manganese Mercury Molybdenum Nickel Selenlum Silv6r Thallium Uranlum Vanadium Zinc 70 70 70 70 70 70 7g 7B 70 70 70 70 70 70 7D 7B 70 130 130 130 130 't30 130 130 130 130 130 130 130 130 130 130 ,130 130 3,1 4.2 1-7 0 2.8 0,3 0.7 't.4 0 0 2.5 4.6 0 1"3 a 5_5 spocilicarlonB. (EPA Mcthod 200.8, PEr. 8.4.4) I Il-' RL %REC Low Limit High Limlt RPD RPDUmII Qual t I Qurlificrs: RL -,{nalyte reporting limit. ND - Not detected at tho reporting limit, A - The anallte level was greater than four times the spike tevel- ln eccordance with the method % recovery is nor calculated. S - Splke recovery oulslds of advisory limits" Jun-Zi-05 I l:36am From-lUC BLANDIN0 801 6tB 2224 T-7s4 P.832/s56 F-41 5 ENEBGT LAaoRATonES,.tNc ' 2393 Satl Cree* Highway (8260/) - Po. 1ox 3QQ ' Casper; W8#02 Tc11Frce888.235.0515 , 307.2 fl, . Fax 307.234-/639 ' casper@eneryylab.cc YwwBneqytab.con QA/QC Summary Report Client: Internadooal Uranium (USA) Corp Project: lst Quartcr POC SamPling Report Date: 04/I9l05 Work Order; C05O40027 t I I I t I t I I I t I I T T t I t I Anelyte Result Units RL %REc Low Limit Hlgh Limit RPD RPDUmit Qual Method: E353.2. Sample lD: MBLK-1 Nihogen, Nlrme+Nihite as N sample tD: C05040027{05BMS Nltmgen, Nitrat€+Nltrllg as N SamplelD, G05040027-005BMSD Nitrogen, NltraterNitite as N Sample lD: MBLK-17 Nltrogen, Nitrate+Nitrite as N Sample lD: C0504002&009BMS Nltrogen, Nitrats+NlrlB as N Nilrogen, Nitrate+Nitrrte aS N Sarnpte lB: MBLK{z Nitlgsn, Nihate+Nitrib as N Sample lD: C050400834018MS NitrEgen, NitraP+Nltrlte as N Sample lD: C0504008I!-001BMSD Nltrogen, Nihate+Nitrite as N Sample lD: MBLK-{8 Nlhogen, Nitrete+NiFia as N Meihod Blank . ND mg/L Matrix Spilte 1"87 mg/L Matrlx Spike Duplicate 1.83 mg/L Method Blank ND mg/L Malrix Splke 3.30 mg/L 3,30 rnglL Method Blank ND mg/L M8trix Spike 4.46 mg/L Maflx Spike Duplicate 4.51 mg/L Mehod Blank ND ms/L 0.03 0.10 0_10 0.03 0,10 0.10 0-03 0,1 0 0.10 0.03 11090 Batch: A2005'M-05_1 _NO3_01 04/05/05 1O:59 04/08t05 11:18 04/05/05'11:19 2.2 10 04/05/05 1 1 :sg 04/05/05 11i54 04/05/05 11:56010 04105105 12t16 Ml05l05 12234 04/05/05 12:36 10 04/05/05'12:59 9't.5 fia -.,] ,i i -'t sample lD: C05040028'00SBMSD Makix spike Duplicate 1,111090 Method: E900.'t Sample lD: C05040098.00'll Gross Alpha mlnus Rn & U Sample lD: C05040099-00{l Gross Alpha mlnus Rn & U Sample ID: M8fi48727 Gross Alpha mlnus Rn & U Sample,D: LCS-R48727 Gross Alpha minus Rn & U Sample Dupllcaie ND pCi/L Matrix Spike 40.0 pCi/L Method Blank ND pCi/L Lahoralory Control Spike 37-B pCl/L 106 1-0 1.0 Batoh: R48727 06/05/05 1 1:45 30 04/0s/05 11:45 04/05/05 11:45 04/05/05 -l 1:45 701001.0 130 Quolificra: RL - analyte reportlng limit,ND - Not deiected at the reporting limit. I I Jun-ZI-05 ll r36am From-lUC BLANDIllE 8gl 618 2224 T-7S4 P.033/056 F-415 ENEBGT LA1OfrATaFIES.,NC, . 23e3 Salt CreekHbliway (s200U 'CO. Box 3!5Q ' Ga.sp€c Wv82602 Toil Free 888.235,0515 . 307.2' yl5 ' Fdx 307.234.1659 ' casper@enargylab-cc Ywulenergytaa-con I I t I QA/QC Summary Report . I Sampla ID: 06-APr'05-LCS-3 I AcetoneI B"n="nt Laboratory Control Spike 54 ugil5.0 uglL 5.1 uglL5.0 ug/L'5.5 ug/LI'g ug/L53 ug/L5.0 ug/L3.8 ug/L4.4 ug&4.8 ug/L Repori Date; 04119105 Work Ordcrt C05040427 Otl06l05 11i37 04/05/05 14:39 Cltent Interuatioaal Uranium (USA) Corp Project: lst Quaner POC SamPling Method: SWBZ60B Iri .! -l 130 130 130 '130 130 130 130 130 130 130 130 120 4aE 124 120 I I I I I 94.4 70 130 106 80 12097,6 70 125 92 80 12098.4 80 120 ti I ,-l li Carbon telrachlodde Chlorsfrcrm Chloromethane m+p-Xylenes Methyl ehyl kerone Methylene chloridE Naphthatene o-Xylens Toluene Sum'1,2-Dlchlorobenzened4 Surn Dlbromolluorcmethane Surr p-Bromofl uorobenzene Sun': Toluene4S Samplo lD: 0E-APr45-LCS-4 TefiEhydfofuran Sur: 1,2-Dichlorobenzened4 Su n-' Dibromgfl uoromethane Surr: p-Bromofl uorobenzene Sur: Toluene'd8 Sample lDt 06-Apr'05-ltlBLK-B Acetone Benzene Carbon ialrachlorlde Chlofilform Chlorcmehane ryr+p-Xylenes Merhyl ethyl ketone Merhylene ohloride Naphthelene o-Xylene Tetrahydrofuran ToluBn6 Xylenes, Total Sun: 1,2-Dichlorobenzens-d4 Sun: Dibromofluortmethane Sun: p-Brornofl uorobanzene Sun: Toluene.dE Laboratory Control Splke 47 uglL Method Blank NB ugll ND ttg/L ND ug/L ND ug/L ND ug/L ND ug/L ND ugiL ND ug/L ND uglL ND uglL ND uS/L ND uglLND r.lg/L 20 1071.0 100 1.0 102 {.0 1001.0 1101.0 98,820 108't,0 '100 1.0 7e-e1.0 881,0 961.0 1011-0 97_2 1.0 1001.0 1A2 70 70 70 70 70 70 70 70 70 70 70 80 70 EO 1,0 1.0 1,0 1.0 1-0 10 0,5 0.5 0.5 0.5 0-5 10 0.5 0,5 0-5 0_5 0.5 0.5 0-5 1020.5 93.20.5 840.5 102 80 120 70 125 80 120 B0 120 Result Unib RL o,6REC Low Limit Hish Lirnlt RPD RPDLimit oual iIj I II]I l I, ND - Nol d€t6cred at rhe reporting limit. Qulliticrr: RL - Analyte reportlng llmit, I i Jun-27-05 11:36am From-lUC BLANDIlrlG 801 678 2224 I-ts4 P.0341056 F-415 t ENEBOy LABoRAToPlEg.INC. , 2393 Sall Creek H4?hway (8260t)'RO. Box 3258' casper, wr8260- To11Free888.235.0515 , 307.2 Yl, ' Fax 307.214,/639 ' casper@eneryylab,co Ytueneryylab.con Ir l QA/QC Surnmary Reportt I ;:'.:::, flffi'J.Tixfffilll,**Report Date: 04119105 lVork Ordert C05040427 li I .ltr I I T ll Ir Analyte Resulr Units RL %REC tow Llmir Hish Llmlt RPD RPDUmit Oual Method: sWSztoB Sample lD: 0B.Apr-tl5-MBLK-8 Sample lD: C05040027{03AMS Benzene Carbon tetradtlodde Chloro6rm m+F-Xylen6s o-Xylane Toluene Sun: 1,z-Dichlorobe nzene-d4 Sun: Dlbromofl uorometha ne Surr: p-Bromofl uorobenzene Sun: Toluene{E Sample ID; G05040027-003AMSD Benzene Carbon tebachloride Chloroform 6+p-Xylenes o-Xylene Toluene Surn 1,Z-Dichlorobenzansd4 Sun: Dibromofl uoromethane Surr: p-Bpmofluorobenzene Sun: Toluene'dB Method Blank Matrix Spike 430 uglL 480 ugfl_ 660 ug/L 530 ugll 530 ug/L 44o ttE/L Matrix Spike Dupllcate 4S0 ug/L 490 ug/L 870 ug/L 540 ug/L 530 ug/L 470 us/L 25 86.8 70 '130 25 91.2 70 130 25 E6 70 13025 107 70 13025 105 70 13025 88.8 70 13025 103 B0 12025 98 70 12525 91,2 E0 12025 s6_8 80 120 25 97,5 70 13025 97.6 70 13025 88.4 70 13025 107 70 13025 105 70 13025 S4-8 70 1302E 1A4 80 12025 97.6 70 125?5 88 80 12025 104 80 120 12 6.8 1.8 0.4 0 6,5 0 0 0 0 Batch; R48595 0l/08/05 14139 04/06/05 20:46 04/06/05 21;32 20 20 zo 20 20 20 10 10 't0 10 li I I,j I I j Qualiflerr: I i RL - Analyte reportins lirnlt. IiI ND - Not detecied at the reporting timit. - Jun-27-05 l1:3lam From-lUC BIANDII{0 801 878 2?24 T-7S4 P.035/055 F-41 5 I@,If FZ!{,iih?Efl?5!82t4'7'i,'!'#'jlg5;lip*-:uyfJa;E&yr,:i#5#::#&trJff r @ --- -- ! I -'I1 N.Il b; -l ' L,f Ioil),tr L -:l oi!?a-ldJoflrrx,:ta.Jw llPttr Yil;fCtrE*E -a?lll/,,',P ioioE:.l $ 'Aa-=rtrfi-iI ,_i g35E=LdIEio >r.E?rIE ."1 ffiE!o -E)E lo-eE =Era^lurloifi Ild Iit I I I I I I I t t I I I I I I I I,l l, I zzz ,J 2 tt, o.E HE !:tE,o*uor0 -'tsa{ N Ihits.9 t\ IrI a itF.l t:$ -En J ,\F -.l, o .L -!l E'a=ciE=EEdo x-E A- O -Eofi88>\ uJ troq6 HIE2 ?618D (IVl) punoEuJnf Hsrlu r€qlo- IefeEots- xuollqeEef sp1o5p1;og.le1effi .r;p IOEASn V:sd,(IotdurEs e sreursluoclo regunN E sl- h. J E-3 J')xt..$-\a.lc?o uXFE o o CL-o iJrEUo>E-oE ll,9'r; J -'i d f e- nsP <(t= JCL (\lH€ <ri5 rlE 8Hn B:8 p Q op E E Eq.E,6 il=,r, Jun-27-05 1 I ;3lam From-lUC BLANDING B0l 618 ??24 t-784 P.036/056 F-4r5 ENERGY L./|BOFA1OBIE5,. t4C. . 2393 Satr Creek Hishway (02501) ' PO, Bax 0!-5Q ' casPel yw 8!602 To// Free 888.235.0515 , 307.2 tf 15 ' Fax 307.234.1639 ' caspar@energylab.co ,fwwener1ltat.ctn Jol*t llza=I^EGffi O4^lS},lEdt E € e3t3ffi[Essr-6 lo lE toEaE r,l Fl\l|\x ?\3 \ ^r19 I *\9 hrs> .J\t\F\ iA rulcl:E.9 B,l 'qEEIEPdI P5e I E.EfiI*r-Ll . -E(trt_.dE sr I#g3 HIE E -F€ I.! - l--.---ra [IVI]punoreurnJHsnu O3H9VILV:l=ls P^\EBI dlcRD ('4S J€UIE- ,(EsseolE X uopela6a6sp;logTstlosrereivt.rI? E 6 E 1511i1Y:oddl atdures EsJaulEuo3loragunN E o =0(Jcal .:o'o :_; ql ...-o j - L{l I-oo) IE,l- I I T I lEirl a, llEll+lloil; Il p,tt€IEIrEld, U)l.c .YIE€le* "5lE, dl(JlEleib l€; aiI5E EI tr!El-iE aLIEE6 IE; BlE ].elE! e IEiE IEE Elo>-= ls! 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BN 5256. - Casper; WaE802 TollFrcea98.235.05l5 ' 307.2 JrU ' Fpx 302234.1635 ' casPer@energylab.co .Trww.energilab.con .iI i.rrn l,dI. .'-l drp.)a'-5 a>ofl :B g&i 'rt I=t, 2 t2 ,?r)E -!L'X Drfl* ,-,- 8 -^G:D*l'J il >rd, EEto,ra--rE EgiE;f4Ef=,I,L'0) rc -t !,?E D'= IQ6*pErr I.EH I 5El,76- I I I t I I I I I I I I T EEEg6E=0 t) a, EeoE o (!oo o,r G'z otr .E Eol!o l---ol!ooIJ oE.o tr o D(L E o& Loll -E' 0)'56o)trtoeot 1l {5 I @D0)Ero Ctoo e o o o o t =L'o> o6 o0'; J -6 Ts trsg <o= Jqg NE€<llt'E.=OE tdL) 6qt ()EF5o.t ulqq Z > * J-t J ^"$I,J \o \N A &d d \l:..Jj IJ o EIt I :;Ui& r>'av E: rl_-u 4p\ Z.t,rJ,g HE FO>+r&o E o EILIIE.o orJU1 =EI5s=l STEI:etl.9a'l -tr(s1.-dE*lEgfr PIE: -e-5 l,qr= tv!,, LwIJ punorEurnl Hsnu r.lN{ I ^TL\.! \ .ir r\ d i qS :ar4[ Ai:eseorfr X uopara6efr rpllogTenog ra1efr .r1! [ 881 Ell Z??4 T-is4 P.0381056 F-415 ENEFqY IABOBATOfrIES,-INO. ' 2395 SaltCreek Highway (02601) ' P.O. Box 335Q ' huPo,; WW002 TolFreeSSS-235.0515 ' 30zI \f/5 ' fvx 307234.1639 ' casper@enetgylab.cc ..yww:energylab,mm .\id ,I^ ,\ol\-lo --tl = l.lEN 6rr =& n._R=+ is I I zzzI 'l dE> :*lii5eHg s t6:I L - -{-o .l i: -r r #Hsqg-hlssFE HS IUEf-oo)a:= ca'13:ilE€e I-e \Jt SEetr€ 3!,(a a @ LLVIJ punorEurnl Hsnu l\{i. ,rorll0 fiesseolg x uog1E{sBBTlsp1os/stto$rqem{y E Oatrg116y:ed,toldurcS EsreulquoC lo raqurnN = o =EOr@,! o'o EeSs f $a 56e=o I.ljrla ll i; ll ="Is llElI 6lt>|lEolEEIE .iEl: t;lg ;-lEr EleI EILE>td_l.E,r! 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H-tr-l fE#l'E lEz: IQ.its c I EE slt 5EE I.5 ur (.fVjJ punorBurnf HSnU d NNIrhB 1' 6E E J6qt6 ,G66EolE Xuogqa6aftsp11o57a1og.rapffirB frOeASnAV:BdI1e1dure5 tsraulrluosroJsgurnN = EeSx f BE E6E=ttt I ! Jun-27-05 ll:37am From-lUC BIANDIN0 801 67A 22?4 T-7s4 P.040/056 F-415 t- -:; ENEfrGy L/lBORAlpilES, !!!C. . 23e1 Salt Creak H$hwey (826O1) . P_O. tur sry , CaspsE Wv826Az - fflNflF{efd TollFree 888.235.05/5 . 3022'-Yrs , Fax 307.234.dJ9 -'cispvdeneryylab.cc ''\mrehergylab.con I t t I T-D( * @t lr'4 h-o.! fr a1 l, l5 ,lt *tifiJ;I G ,i'- t- I Jun-?i-05 I I r38am From-l UC BLAltlDING 8A1 678 ZZ24 T-i84 P.CI411056 F-415 ENERGY IABORAYOBES, lNC. ' 2393 Sdli CreeA' l'tilhway (82601) ' EO. 9ax 3?5Q ' Caspe4 WY wN3 TollFree888.235.0515 , i07.2 yrt . Fax 302234.1639 .'casper@energylab.cc 'ywwenxgylab.conI I t t n T I I I I I I I ctient Name lnternational Umnium (USA) Corp '*'Work ordet Number CO6O4OO27, ._i rI ]checktist completed uv: t ; FUeri- <-l- l *rfffi,,".^^_-re- Energy Laboratories lnc. * Shipping container/cooler in good conditlon? I lCustody seale intaci on shipping conlalner/cooler?.i Custody eeals intac-t on sample boltlas? j Chein ofcusrody present? ' - Chaln of custody signed when retinquished qnd received? ' r Ghain of custody agrces with sample labels? It Samples in prpper contalner/botile? ., Sample containers lntact? ,__ I Sufticient ssmpls volume for indicaled tesl? All samples received wlthln holding lime? i Gontainer/Temp Blanx t€mpereture in compliance? watar - VOA vials have zero headspaca? ] warer ' nn acceplable upon receiPt? Adjusred? Sampla Receipt Checklist Carrier name UES Date and Time Reseived: Ll1l20O5 l0:15;00 Received by las Raviowod by ll YeE E Yes E ves fl yas E Yes M Yes E Yes E Yes n Yes EI Yes El ves EI Yes EJ Yes M ruoE ruoD ruoE ruoE No fI tto E Non tlo M ruon Nsn woE xoD NoE Cheoked by Not Present I Not Present I NotPresent E 3,8 "C On lco No VOA vials submllted Not Applicabb n '1 I Any No and/or M (not applicable) rdsponse musl be detailod in lhe commenis section below, I I 1 Client contac{ed , Contacled by: Daie contacied: Regarding: Parcon conlacled i; Comments: 2 viqls tqr serrlple MW14 received at lab-broken. IiIII f .--] "**"iveAction li i l,i F^r n ^4- n^E^ I : Jun-2i-05 l1r38am From-IUCBLANDING 801 6t8 ?224 T-is4 P.s4?/s56 F-415 I ENERGY LABORATO1ES,-WC. '2393 Satt Oeeh'Highwav @m?il'PO. Box 3255. ' Cdsryt WY826v! To/1Free888.235.0515 , 307i' \/5 ' Rx 307.234./635 ' caspEr@eneryylab-cc .Ywwensryytao'com I III i D*er l9-ipr-AS ; I I CLIENT: falsmari6nal Uranium OSA) Corp I -- Project: lsrQuanerPoC Sampling CASE NARRATIVE ,, i Sample Dellvera Group: CA5040027 lj I T I I I I t I THIS IS TITE FINAL PAGE OF TI{E LABORATORYANALYTiCAL REPORT BRANCH LAB ORATORY LOCATIONS eli-b - Energy Laboratorieq Inc. - Billings, MT eli-f- Energy Laborarories" Inc- - Idaho Falle, ID eli-g - Energy Laboratories, Inc. - Giilerte, WY eli-h - Bnergy Laboratories, Inc. - Helena, MT eli.r - Energy Laboratories, Inc. . Rapid City, SD eli-t - Encrgy l:boratories, Iuc- - Cbllcgc Station, TX oRIGINAL SAMPLE SUBMITTAL(S). A11 original sarnple submittals have bees reumed wirh rle dara package. A copy of the submitul(s) has been included and tackcd in the data package- SI.]BCONTR.{CTING ANALYSIS Subconiractiug of sauryle anaiyses !o an outside laboratory rtrBy be requircd. If so, ENERGY LABORATORIES qrill utiiize its branch laboratories or qualifred contrsct Ieboratories for *ris service- Auy such laboratories will bc indiqsred within the Laboratory Analyricai Re,port. SAMPLE TEMPERATIJRE COMPLIANCE: 4oC (*2"C) TeryErarure of samples receivcd m"y not be considered properly preserved by accepred star6*45- SemFlcs thar are hand delivcrcd immediately after collectioo shall bc considered acceptable ifthere is evideace tlat the chilliug process has begu- EMRGY LABORATORIES, INC. - CnSpgR,*Y ccrtiEes that ccrtain rrcthod selections contained in this repon meer requiremens as ser f,orth byNELAC. Sornc clico.t specific reponing requiremeffs may not require NEISC repordug protocol, NELAC Cenification Nurrrber EE764l. ELI appreciatcs fhe opportuniry ro provide you wirh this analytical scrvice. For additional fuformation and services visir our web page wwuenergylab.conr. The roul nurnber of pages of this repofi are indicated by the page nnlnber locardd in the Iower right comer. 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Caspes W836V3 To/1Free888.235-0515 , 307.2 ytt , Fsx 307.234./639 ' casper@enargytab.co v,ww.energylab,conI I I t I ANALY TICA L S UMMA RY REPORT April 19,2005 David Turk lolsrndignal Uranium (USA) Corp 642s S Hwy 191 PO Box 809 Blanding, UT 845I I Workorder N a -: C05040A27 FrojecrName: lst QuarterPOC Sampling I Energy Labomtories Inc. rcccivcd the followiqg 6 saurples from Intcrnatioral Uranium (uSA) Corp on 4llt2015 for anhlysis. Sample II)ClieutSample ID Collect Date Receive Date Matrix I T t c05040027-001 Mwl l A3B0/05 12:18 04101105 Aqueous lvfetals by ICP/ICPMS, Toml Chloride Fluoride Ninogen, Ammonia Nitrogcn, Nitrote + Nitrir Metels Digcstion by EPA 200.2 Gtoss Alpho minus R1222 snd Uranium Solids, Toral Dissolved Suliare SW8260B VOCs, Extended List c05040027.002 Mwt4 03/30/05 10:57 04/0I/05 Aqueous Same ds,lrbove I c05040027-003 Mw26 03130105 10:15 04/01/05 Aqueous Same As Above c05040027-004 Mw32 03/30/05 13:14 04101105 Aqueous SameAs Above c05040027-005 Mw60 O3BA|05 093O A4lQl/05 Aqueous Same As Above c05040027-006 Mw63 0?l3O/05 l2:18 04/01/05 Aqueous Same As Above I t There were no problems wirh rhe analyses and all dara for associared QC mer EPA or laborarory specificariorn except whcrc notcd in thc Case NErretive or Report, Ifyou have any quesrions regardif,g rlrese tests results, please coll. /r/Repon Approv ed B>-{r-€ Czff;;; - Oret,fvAsgunatrcEDtFEsoR I I Ir t I I Glacier David Frydenlund Page 1 of 1 From: David Frydenlund [davef@intluranium.com] Sent: Thursday, June 30, 2005 4.21 PM I ]1r"",, ff[ [,::]ffiI,,,, etr 2005 Groundwater Monitoring Resurts t Dear Mr. Finerfrock, I We have sent two copies of the White Mesa Uranium Mill Groundwater and DMT Performance Standard Monitoring I Report for the 1st Quarter of 2005 to you by Federal Express this afternoon. I l, ?-.::ldrn"e with Part l.F '1.e) of the Mill's Groundwater Discharge Permit, attached to this emait is an etectronic copy of! all laboratory results for groundwater quality monitoring conducted, in Comma Separated Values (CSV) format. t Yours truly, I David C. Frydenlund I Vice President and General Counsel t I t I I I I I slot2oos lr I I I I I I I T I I White Mesa Uranium Mill 1st Quarter 2005 wastewater Elevations cells 1 and 3, feet above mean sea level 1t7/2005 1t13t200s 1t19t2005 1t2712005 21212005 2/1012005 211712005 311t2005 3t9t2005 3117t2005 3124t2005 3t31t2005 Cell#1 5612.34 5612.s4 5612.49 5612.6 561 3.1 3 5613.56 5614.27 5615.01 5614.99 5614.88 5614.86 5614.84 Cell#3 5600.64 5600.99 5601 .1 3 560'1.37 5600.2s 5599.07 5597 44 5595.43 5597.32 5598.6'1 5599.56 5600.42 I t ll li ll ll li I t I I I I I I I I t I I t I I I I t II i White Mesa Uraniurn Mill 1't Quarter 2005 Wastewater Elevations Roberts Pond, feet above mean sea levelI 1 I 't 1: I lI 't l Date 3l09t0s 3117/0s 3124/05 3B1lA5 Wastewater Elevation (fms]) 56i 8.55 5618.70 5618.80 5618.79 I !)