DRC-2006-001143 - 0901a0688080569c

THIRD QUARTER
RADIONUCLIDE EMISSIONS TEST
COI\DUCTED AT
INTERNATIONAL URANIUM (USA) CORPORATION
NORTH YELLOW CAKE SCRUBBER
BLANDING, UTAH
September 14-15,2006
by:
TETCO
90 East Main
Lehi, UT 84043
Phone (80r) 768-0973
Fax [phone]
- Date of Report:
:- October 2412006
Prepared for:
International Uranium (USA) Corporation
6425 S Hwy 91
Blanding, Utah 84511
CERTIFICATION OF REPORT INTEGRITY
Technical Emissions Testing Company (TETCO) certifies that this report represents the truth
as well as can be derived by the methods employed. Every effort was made to obtain accurate andrepresentative data and to comply with procedures set forth in the Federal Register.
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TABLE OF CONTENTS
Introduction
Test Purpose
PAGE
Test Location and Type ofProcess .
Test Dates
Pollutants Tested
Test Participants
and Methods Applied
Deviations From EPA Methods
Quality Asswance
Summary of Results
Emission Results
Process Data
Description of Collected Samples
Discussion of Errors or Inegularities
Percent Isokinetics
Source Operation
ProcessControlDevicesOperation ......5ProcessRepresentativeness ......5
Sampling and Analysis ProcedtnesSamplingPortlocation.... .....6SamplingPointlocation.. ......6SamplingTrainDescription. .....6
SamplingandAnalyticalProcedures .... .......7QualityAssurance .......7
Appendices
A: Complete Results and Sample Calculations
B: Raw Field Data
C: Laboratory Data and Chain of Custody
D: Raw Production Data
E: Calibration Procedures and Results
F: Related Correspondence
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Table
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II
m
TV
LIST OF TABLES
Measured Radionuclide Emissions
Percent Isokinetics
Sampling Point Location
Complete Results ...AppendixA
LIST OF FIGURES
Figure
1 Facility Schematic Representation . . . . Appendix D2 Schematic of Method 5/l 14 Sampling Train . . Appendix E
- INTRODUCTION
- Test Purpose
This testwas conductedto determine thetotal radionuclideemissions fromtheNorth yellow
Cake Scrubber exhaust in terms of Curies per dry standard cubic foot (Cildscf).
u Test Location and Type of Process
Intemational Uranium (USA) Corporation is located about 5 miles south of Blanding, Utah.
- Uranium ore is processed into yellow cake, which is shipped to other facilities for additional
processing. There are two yellow cake dryers with individual scrubbers. The North Yellow Cake
dryer was the only operating dryer at the time of the test. The South Yellow Cake Dryer is currently
- not operational.
A facility schematic is shown as Figure I in Appendix D.
Test Dates
All testing was completed September l4-15, 006.
v
Poilutants Tested and Methods Applied
The tests were a determination ofradionuclide emissions in accordance with EPA Method
5/1t4.
Test run filters and front wash residues were sent to Energy Laboratories in Casper Wyoming
for radionuclide analysis.
Test Participants
Test Facility Wally Brice
David Turk
State Agency None
TETCO Paul R. Kitchen
Joseph Kitchen
Deviations From EPA Methods
None
- Oualitv Assurance
Testing procedures and sample recovery techniques were according to those outlined in the
- Federal Register and the Quality Assurance Handbookfor Air Pollution Measurement Systems.
:
SUMMARY OF RESULTS
Emission Results
Table I presents the findings of the test in Curies per dry standard cubic foot. Table fV inAppendix A has more detailed information.
Process Data
The process was operated according to standard procedures. All pertinent process data wasavailable for recording by agency personnel. Scrubber water flow *d prrrr*, readings were
recorded and are found in Appendix D. Production data will be submitted bylnternational Uranium.
Description of Collected Samples
All test filters were lightly covered with a yellowish colored particulate. The front washes
were clear in appearance.
A second run was attempted on the 146 but approximately 168 minutes into the test a high
vaculnn caused water to be drawn from the first impinger into the filter holder. This voided the run
and no attempt was made to recover any portion of the sample train. A successfrrl third run was
completed on September l5th.
North Yellow Cake Scrubber
6.986E+05
9.6438+05
Percent Isokinetic Samnling
Each ofthe tests were isokinetic within the + l0% of lXI%criterion specified in the Federal
Register. They also meet the Utah State Department of Environmental Quality, Division of Air
Quality specification of isokinetic sampling point by point. Isokinetic values for each test run are
presented in Table II.
SOURCE OPERATION
Process Control Devices Operation
All process control devices were operated normally. Recorded scrubber water flow and
pressure readings were recorded and are found in Appendix D.
Process Representativeness
The facility was operated normally. Production data will be submitted by Intemational
Uranium.
Sampling Port Location
The inside diameter of the North Yellow Cake stack is 18.0 inches. The two, four-inch
diameter sample port are located 6.3 diameters (9.5 feet) downstream from the last disturbance and
6.3 diameters (9.5 feet) upstream from the next disturbance. Figure I in Appendix D is a schematic
of the stack.
Samnling Point Location
Table III shows the distance of each sampling point from the inside wall according to EPA
Method 1. Each point is marked and identified with a wrapping of glass tape and numbered. These
points are determined by measuring the distance from the inside wall.
Sam Point Distance
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2
aJ
4
5
6
7
0.58
1.89
3.49
5.81
12.t9
14.51
16.11
Sampling Train Description
To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods l-
5/ll4werc followed.
All samplingtrainsweremade ofinertmaterials, (Teflon, stainless steel andglass)toprevent
interference of the sampled gas and particulate.
The stack analyzers used to conduct Methods l-5/ll4 are constucted to meet the
specifications outlined in the CFR. The temperature sensors are K-type thermocouples. Heater,
vacuum and pitot line connections have been designed to be interchangeable with all units used by
the tester. A 316 stainless steel probe liner was used for the tests. Figure 2 in Appendix E is a
sketch of the Methods 5/l l4 sampling train.
Sample boxes were prepared for testing by following the prescribed procedures outlined in
Methods 5/114.
Sampling and Analytical Procedures
All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A,
Methods 5/114.
Ouality Assurance
All equipment set-up, sampling procedures, sample recovery and equipment calibrations were
carried out according to the procedures specified in 40 CFR 60 and.the Quality Assurance Handbook
for Air Pollution Measurement Systems.
APPENDIX
A: Complete Results and Sample Calculations
B: Raw Field Data
C: LaboratoryDataand Chain of Custody
D: Raw Production Data
E: Calibration Procedures and Results
F: Related Correspondence
APPENDIX A
Complete Results
Nomenclahue
Sample Equations
A
eMb
NqlhYdlq€k€
TABLE IV
COMPLETE RESULTS, RADIONUCLIDES
INTERNATIONAL I.JRANIUM CORPORATION (IUC)
NORTH YELLOWCAKE SCRUBBER EXTI,AUST
DimensionsSymbol
Date
Filter #
Begin
End
Pb.
AH
Y
Vm
T-
{ap
Wt*c
T,
ce
Do
Coz
o2
N2&CO
Vmoa
Vw
Bw.
xd
Md
Ms
Yol
T"
As
PG
Pbo
P.
Q'
Q"
vs
Curies
Crad
ERrad
Description Run #l
91r4t2006
4800
8:44
l2:00
24.35
1.354
1.002
143.146
9t.2
0.3047
550.5
r92
0.84
0.3715
2.00
17.80
80.20
112.275
2s.9s6
0.1 39
0.861
29.03
27.50
99.8
119.3
t.767
-0.03
24.28
24.278
1.388+03
2.t6E+03
1.22E+03
950.0
8.461
6.986E+05
Run #3
9/15/2006
4802
8: l7
I l:54
24.30
1.431
r.002
r46.167
82.5
0.3177
603.4
192
0.84
0.3715
1.80
18.00
80.20
rt6.272
28.450
0.r37
0.863
29.01
27.50
98.9
I 18.6
1.767
-0.03
24.23
24.228
1.44E+03
2.25E+03
1.28E+03
1300.0
I l.l8l
9.643E+05
Date
Time Tcst Bcgan
TimeTest Ended
Meter Bilometric Pressue
Orifice Pressue Drop
Meter Calibration Y Faaor
Volune Gas Sampl€+-Mets ConditioDs
Avg MeterTempenhre
Sq Root VelocityHad
Weight Water Collecled
Duration ofTest
Pitot Tube Coefficimt
Nozde Dimoter
Volme % Cabon Dioxide
Volm 7oOrygm
Volrm % Nirogfl md Cubon Monoxide
Volme Ghs Sampled (Stadad)
Volw Walcr Vapor
Fractim H2O in Stek G6
Fnctim of Dry Gas
Moleolar Wt. Dry Gas
MolmrluW. StrckGd
Percent Isokinetic
Avg Stack Tmpenhre
Stack Cross Scctional Area
Stack Static Pr6src
Sample Port Baromeric Pressure
Stack Prcssue
Stack Gas Volwtric FIow Rate (Srd)
Stack C8s Volmetric Row Rate (Actual)
Velocity of Stack Gd
Radionuclides per smple
Concmaatim of Radionrclides
Emisaon Rate of Radionuclides
In. Hg. Abs
In. H2O
dimmsionless
cf
r
Root In. H2O
Gmm
Minules
Dimensisrls
Inches
Perctrt
Ptrc€nt
Pscflt
dsf
scf
Fraction
Frutim
lMbnol
lb/lbmol
Perc€nt
T
SC. Ft.
ln. H2O
In. Hg. Abs
In. Hg. Abs
dscfin
cfrr
Sm
pci
pCild$f
pCi/lr
AVG
119.0
1.41E-r-03
2.218+6 ;$
1.25E+03 J-Y
9.821
83r48+05
Saturat€d moisture fraction used in all calculations for runs I & 2 as the measured moisture was supenaturated
\A _{+}6 a.AE'+3
t.e5f+9\: :
V ' f-fh"^,ul^ia lf"
IQ** \rn,
4
-rupr.l bc:f,cr
u'^ t)'glt** 7
\ u):tr^i!
5.t,
M5 Nomenclature
o/ol: percent isokinetic, percent
As = stack cross-sectional area (ft3)
ASAP = see {AP
Btu = unit heat value (British thermal unit)
B* = fraction of water in stack gas
Cs = cono€lltration of particulate matter, back half (grldscf,lb/dscf, etc.)
Cs= concortration of particulate matter, front half (grldscf,lb/dscf, etc.)
Cmetat = concentration of metals (pp-, t g/ft3, etc.) atomic symbol replaces "metal,'
COz= percent carbon dioxide in the stack gas
Co: pitot tube coefficient (0.84)
Cx @"d: species symbol replaces x.
Cx ("o,,) : acfual'gas concentration corrected to required percent 02
AH: orifice pressure drop (inches H2O)
AHg = orifice pressure (inches H2O)
AP = 51ask flow pressure differential (inches H2O)
D, = diameter of the stack (feet)
Dn= nozzle diameter (inches)
EA: percent excess air
ERs = emission rate of back half particulate (lb/hr)
ERF: emission rate of front half particulate (b/hr)
ER -s. = emission rate per mmBtu or ton of fuel etc.
ERx = emission rate of compound which replaces x
k-fact = multiplier of test point AP to determine test point AH
L = length ofrectangular stack (inches)
mlltu = thousand Btu
M6 = molecular weight of stack gas, dry basis (lb/lb-mol)
Mp = rlasS of particulate on filter (mg)
Mpp = lnoss of particulate mafter on filter and probe (mg)
mmBtu = million Btu
' M. = molecular weight of stack gas, wet basis (gigmol)
N2 = percent nitrogen in the stack gas
02 : percent oxygen in the stack gas
{AP = average of the square roots of AP (may also be referred to as ASAP)
Pb, = absolute barometric pressure at the dry gas meter (inches Hg)
Pbo = absolute barometric pressure at the sample location (inches Hg)
P6 = stack static pressure (inches H2O)
P. = absolute stack pressure (inches Hg)
Po6 = absolute pressure at standard conditions (29.92 inches Hg.)
0 : time of test (minutes)
Q" = stack gas volumetric flow rate (acfrn)
Q, = stack gas volumetric flow rate (dscfrn)
Qw: wet stack gas std. volumetric flow (ft3lmin, wscfm)
Ts = stack temperature fF)
Tsta = absolute temperature at standard conditions (52Sk)
Tt= see0
M5 Nomenclature
um: mean molecular speed (cm/s)
Vm = sample volume (ft3) at meter conditions
vrrrtd = volume standard (dscf), sample volume adjusted to 68T and29.92 inches Hg.
V,: velocity of stack gas (fpm)
V*. = volume water vapor (scf) at 68T and 29.92 inches Hg.
W = Width of rectangular stack (inches)
Wt*" = weight of the condensed water collected (grams)
Xa = fraction of dry gas
Y : meter calibration Y-factor (dimensionless)
Method 5
0/oI : Vmo6 . (T, + 460). rc39/ (0 . Vs. P, . & . Dn2)
A.=(Ds2/4)'n
B*: V* I (Vmr,a +V*)
Ce=Ms.0.01543/Vmo6
Cr: MO.0.01543 /Vmr6
Cx 1"orr;: Cx(u*; . (2O.9 - desired %O2) / Q0.9 - acfialo/oO2)
D.r=2.L.W/(L+W)
Dnd". = ^l 1o.ozee. (pb, + 0.0735) / (T, + 460). ce . xd . {(T, + 460). Mr) / (p, . Ap)l}
EA : (%O2 - 0.5 o/oCO) / 10.264 o/oN2 - (yoo2 - 0.5 %CO)l
ERs = Cs. Qr.0.00857
ERp: Ct. Q. . 0.00857
ER..s, = ERx / (mmBtu / hr)
K-fact=846.72.Dn4.AH6. Cl.xo'.Md.pr.(T,+460)i M..(T,+460).(pb.+aH/13.6)J
Ma = CO2 . 0.44 + Q,2. 0.32 + Nz .0.28
M.: (Ma . XJ + (18 . 8,,)
P,: Pbo + (Pc / 13.6)
Qo = Vr'A,
Q, : Qa. Xd . Ps . Toa / [(Ts + 460). Poa]
Qw: Q' / Xa
Vrrsd = Vm . Y . Trtd . (Pb, + Nl / 13.6)/ [Psa. Gm + 460)J
V, : 85.49. 50 . Cp. {ap. { 11t, + 460)/(p,. Ms)l
v*.: wt*" .0.04715
X6: I -8.',.
APPENDIX B
Preliminary Velocity Traverse and Sampling point Location Data
Particulate Field Data
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Stack Dia.
Ports are
Ports are
18"
9.5'
Rcfercnce: Ott
9.5'
Upstrean from next disturbance
Downstrcam &om last disturbancc
PreliminaryN Y Cake Scrb
Comments:
Facility Intemational Uranium
Stack Identification North Yellow Cake Dryer Scrubber
Date /(5e,0{ 2ab
Barometric Pressure
Static Pressure (Po) ^. o3 in HrO
Estimated Moisture @w,) 4-16 o/o
Sample Height from Ground 70 feet
Traverse
Point
Percent
Dianieter
Distance From:Ports
TD Reference A B c D E F
I 3.2 0.58 0.58 llb,o'l s ,,1 ,ors 7
2 10.5 r.89 1.89 ,OS
,,1 ,o, 0
J 19.4 3.49 3.49 '6 .*J 1 ,to 1
4 32.3 5.81 5.81 -.ro ?"S ,,,. H
5 67.7 t2.t9 12.19 .tz 3 lt? ,r) 7
6 80.6 L4.51 14.51 ,o ,," 3 o" .tt
7 89.5 16.11 16.1I 4.td t tal. 4,n
8 96.8 L7.42 17.42 zl ,o1 b tt! b,r>
Averages:
Ts llB.Q ZFlow rt,l
AP ,otb {ap .}oso
5 Z Flow
AP
KEY:>
5///'/ risra oat" str*t
Plant: Intemational Uranium
O","t trl
TETCOriltel!)}0_ Samplc Box_/_
Location: North Ycllowsakc Dryer Scrubbcr
owtarcc PavI 2 /(,rU.,a
rorar |tlS.tfb/lA.glSto Jt.b+ lQoQ
vage-LorJ Run# /
1)
A
Diamcter _18,,_ port Rcfcrcnce 0.0,
Portsarc 9.5' Upstream from nextdislurbancf,
Assumed Moisturc 4-13 %
Probe &_-- "r__p,r_Nozlc Calibration
,2IJ- .!7t 3rz_ .r7z
lvg D" .3?/f inchcs
caseaetfa3
Consolc 3v-r,l;,*FZ-
AH@ /.b3t inHro
Baromctric pressurcs
ev^ 21.7f inng
Pb, 2q.29 tnHsp(, -. of in Hro
L.rl Ch€k: gI9 E$l
t'tnin O.@3 O.eOO
vtinuga?.Q 7,O
PibrRrr! A@ O,OO
tn{,o ,23 ,L<
watercolteaea 15O .{ g
Timc Sampled , /? 2 min
Revicw 0gg2q t1
9 ( t pl riovoata shcct ri r,",-4 go-l]ETl,'?,. r*--0-
Plant: International Uranium
Ort",Orr:r*oc= t?avl ?-orCll C
Location: Nonh Ycllowcakc D 'cr Scrubbcr
e"g" / o1__-/ Run# ?
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A
Diameter _l8"_ port Refcrence 0.0,
9.5' Upstrum from nexl disrutancr
Assumed Moisture 4-13 o/o
Probe -ZV--"r__yV_
Nozzle Calibntion,t$o .'Eo -itt .7sl
AvgD" .3&f inchcs
c,aseae F47-.-.2_
Consolcy-r"",or7E
^Ha t,bt, inP,2o
Baromotric Pressurcs
Pb^ 2.l.rt tn*s
Pb, 3'l .Zg in:Hg
e,,_-1o.]_ in uro
Ldl Chcl: &s
nt,nh ]?.ota
wans Z2.O
pitonm O.OO
rote .L{
P$!
Watcr Collected
Time Sampled min
Rcvicw
Tnws
Poid
,\fu!
5+Gf1l.<'t
g+"r+r.l
l3:32
t3:75
15, tz
lu:oQ
to bla" ou\ P?ol
,+afi* tu oo
1o bton) 6,1 ,p11uLes
ifrL-r^d Data shect
, rn -1p z.J tl"l?*
"*__zLPlanr: International Uranium
-
on' t5 S.ff
nug" / orJ Run# ?
J\V
A
Diamcter _18',_ port Rcfercnce _0.0,,arE 9.5' Upstreem from ne)(tdistu$ance
last
Assumcd Moisture 4-13 o/o
Probc eJk__--7r__gg!__
Nozzle Calibration
, )V | .3! | = .31e 372
avgo". 37lf inctrcs
Gas eag J'o .3
Consolc 3
"-F"aor-TdAHo l. /.,39, inH,O
Baromctrio prqssures
Pb^ J'/,)e tnHs
Pb, )'f , L3 ;aguPu -'?3 in HroLcntchet: LCg ee$
dt^tn O.oOb O.onr
vrcin*e ZZ.O ?.O
PilorRaro O.OO 0 aO
tnHzo .Z€ ,L<
l4ta.lt ?/t S,o1lg LZ.qo rgq+)aqo
Water Collectcd
Timc Samptcd /? Z min
R*iew /Zf
Location: Nortlr ycllogcakc prygr Sjrubber
Trwe
Pdnr
./z.{,
,t ght lrr^r" -lr\X va,t*5,ve - b[o.lg4"Ar! -tt+rg lt:t{i
o^,'l- D.4t( Tub"s
APPENDIX C
Sample Recovery
Gas Analysis Data (ORSAT)
Chain of Custodv
?
Method:
Run:t.Sampte so* A
Filter Number:
.lgoo
il4PTNGERS'.
FilterNumber:
48ot .
Finalkl
Initial6y
Net 1g1
''.
RINSES
Initials
P'K
r
rotaf k) 55o.9
Frdt--------- ..-.------ -- cHrcr;----- -
I
Initial o
Initials
Final1gy
Initial 1s1
I\lat /-\
RINSES : -'CHrCt,Final
lnitial
Net
Final _r
-s
tMPINGERg
Filter Number:q@>
l::-/'t-L.tl
lnitials
PEr ,
lKFinalGt
Initialtg)
Net 1g1
Total€y (o03,'{
Final
Initial
Sample Box:
iiiNsES'
.Net
HrO
Final
cH2clr
:
pmt ]n{ernot,ona-f uro-,'u,n^.Lo" tio, N. Ytfioa(oke \-..ven 5".Analytical Method___9BS4T_
,.,:i::11*d-
Gas Bag No. J-o3
Ambient r" pT
Operator f?ta
oate nSqfo|
Test No. LGasBagNo.-FJ
Ambient Temp 7 t
Qperator PTtc
oate rtlsufOb
Test No. 7dasnagNo.:F-
Ambient Temp ?.O
Operator 1F.t4.
Gas
RUN
Average
Net
Volume
I 2 3
Acturl
Rcrdiop
Nct Actuel
Rcedine
Nct Actu!l
Rcrdins
Nct
CO,Z.o 2,o ?-o z-o z-o Z-o z-o
Or (Net is Actual 02
Reading Minus Actual
3Oz Readine)./1- 8 t 7.8 t1.g t7g t1-t t78 r7.g
Y2 (Net is 100 Minus
{ctual 02 Reading).80-z 8o'z 8o'z 80.z
Gas
RUN
Average
Net
Volume
I 2 J
Acturl
Rcrding
uit -,\Acturl
) Rcrdioo
Nct Actud
Rcrdioe
NC.
Cot /.8 \UV
Lg t-g t-8 1.8 t-3 /-g
Or (Net is Actual 02
Reading Minus Actual
3Or Readine).
It.ffr,18-o t1.?t3.o | ?.8 r 8.o r ?.o
\2 (Net is 100 Minus
{,ctual O, Reading).(o.z 8o.z 80.?90,2
Gas
RUN
Average
Net
Volume
I 2 3
Aclu.l
Rcrdios
Ncl Acturl
Rcrdirs
Nct Arlurl
Rcedins
Ncl
CO,t.a t,6 f.8 t.g 1-g t.8 t.9
O2 (Net is Actual O,
Reading Minus Actual
lO, Readins).
tq,8 t6.o t?-8 18 .o r?.8 ,8.O r8.a
\2 (Netis l00Minus
{ctual 02 Reading).(o.L 90.L go .?80.L
CO is not measured, as it has the same molecular weight as N2
TETC O ^::"*".T:;;:;"iEI;;:,
9oEastMain,trhi,Utah 84043 r 801-258-09?3 r FAX [phone]
Chain of Custod
Sample Identification Lecovery Date Sample Descriotion
9l14/06 Filter
Probe Acetone Wash
4800 Filter
4800 Front
Gravimetric
EPA Method 5
Gravimetric
-PAMethod 5
-Gravimetric4800 Back Impinger Catch
4802 Filter EPA Method 5
Gravimetric
EPA Method 5
Gravimetric
EPA Method 5
-Gravimetric
9nst06 Filter
4802 Front Probe Acetone Wash
4802 Back Impinger Catch
Filter EPA Method 5
Gravimetric
EPA Method 5
Filter
Front Probe Acetone Wash
Back Gravimetric Impinger Catch
Sampled by:
Recovered by:
Relinquished by:
Received by:
?ot k KlJh^ Date:
Pou( iL t4.A"n Date:
Date: 7-/f-ae
Relinquishedby: / , 4L/, Date: ?-r/y'a/
Received By:
Analyzed By:
Date:
Date:
unless otherwise indicated, all samples remain in the custody of rETCo.
chain of Gustogy. and Analylical Request Record page / ot I
PLEASE PRINT, provide as much information as possible. Refer to conesponding notes on reverse side.
gompany Narn€l
tr", {arn' /,'on " / (,too, rL'r^
,roj€cl Nem3, Pws F, Fetmfi F, Etc.l
a'e\fiil)P's lvy q /
Dlan/ r'n* tl T lt/ft f
:ontact Nemo, Phone, Fax, E-rnall:
W" //y Etr'c1
V3t 67r-)2/t. € 7/-?27r
Samplgr Name lf other ttpn Contactla-/ tr/c/r-,/2 /aa
,0x lat 76(-??7t
lnvoice Addr6ss:
Jarat 4jan,c -/
ELI Quote #:
Report Required For: pOnrulWWfp E DW O
Special Report Formats - ELI must be notlfled prlor to
sample submittral for the following:
Heuc El nzuE LevetvEl
Other
EDD/EDT E Format
eo€
Ei9'5=fi49XFaP.*P flg: djtg,EF.U*:5s
E
MATRIX
A ul L'l ol il EI rl :s It D
o
trJI(J
EulIU
U)
-i(-
E5e
E
E
Notify ELI prior to RUSH
sample submittral for additlonal
Shlpped by:
charges and scheduling Cooler lD(s)
E5o
E
E
q,lE
?- //
"t)r- //' Or/c e
{i. ,ir7'd
AnolYs2
Receipt Temp
, oc
Custody Seal Y Nlntact Y N
Signature Y N
Match
Lab lD
SAMPLE IUb,N I II.IL;Al IUN
(Name, Location, Intoryal, otc,)
Collectlon
Date
Gollecuon
Tlme' ,&0o E'/ lu )?hrlx 6F F //+> 12-, /.L --
' 7"i Dc "k". )5 2
W Y.fu:z t:,'//r-)q/illt 6F Fft,\ /---/. 'i lU
2.-t- Pr"h- )U'
5
6 r[el
7 EI0cA
E
10 :
Custody
Record
MUST be
Signed
R.lktqubh€dby(pdnl): D|tdllno: _ ShDln:,@,& q/>/ae /t2a /U'fu Re.trao Dy (Pm0: Et8lr/ThF: Slgmturo:
R.[nqubtr.dby(p.h0: Drbrlm: s|endl|t:Rsc.ivd by (Fht): Dats/Tlns: Stgnanrc:
Samplc Dlsposal: Rctum to ollent
-
Lab Dlsoosal: \,. LA,EOR.ATORY USE ONLYSample Type: * oifacUoris -
In certarn crrcumrtancor' ""*L:':lJ:i*::""8::griffil5l;aixn*;#:r1]!E*fi 1"":H,r,s::J..t.r*lfijffisor rocom'rera rhc anarveb ."q,"rrca.
Msit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, & links.
APPENDIX C
Sample Recovery
Gas Analysis Data (ORSAT)
Chain of Custody
Lab Analysis
ENER6J LASOR/{TOHIES. rNc.
2393 Solt Crcek Highwoy Be6Ot
PO Bol( 3258 Cmper, W\l gA60?
vaicet 307.235,0518. Tolf Frce voice: ggg.a35.o5l5 . Fox: w7.zg4.t6ggE-nroil Addrress: [e-mail] r visit orrn web page at: www.energyrob.com
Acsfitl,iltE covER SHEET
,o, .frt /'
-
Fox Mrmber:
Connpany:
Fnom:
This FAX contains pqcs includiry this coven sheet.Z
DATAf PRELx,l rNARy
The foltowirg doto has not bqen proofed for emors nor has doto been reviewed by grnlity ossuronce/grnlitycontrol personnel.
tr DArA REsuLrs
4kiffio
Qrntity ossurcnce/gunlity control persor*rel haw proofed the following doio for errors.
o TH EP, I r N F O R ti 4rr o N R E Q U E s r E D
Cqtfidllttidrry Stotcncnt
This focsinilc til?ssogB Gontoins infurnnfion frcrn Encrgy Labomtorics, fnc. ard rmy be confi&ntial or prMlegcd- The infornotion is irtan&d lobe fon the u$ of the irdiviri|El or entity m|rd obovu' ff you ore mt the intardcd ftcipicht, bc omrc rhor aly disclosrc. copying, distrihdion oruse of thc conf"nts of this l|tc33o9a is prohibiled rf pr received fhis et:ctronic rnesogc in error, pleose notify rs irnrnrfictity uy rcpV fox oefelephone ol l-88E-23S0515.
Revised 07-17-Ot
LABORATORY ANALYTICAL REPORT
Cliont Intenretional Uranium (USA) Corp
Sits Narre: Not lndicated Report Date: 1O24lOo
Lab lD: C06091296-@l
Gfient Sample lD: Filter 4BCD combined with Beaker 24Matrlx: Filter
Gollection Date: 0914/(}6
IlateReceived: 09i26/OB
$cuAndysesResult Unlts eua$fter RL OCL llethod Anatysb Oats, By
RADIONUCUDES . TOTAL
Uranium. Adivity 950 pcilFinet 0.2 St/t/6020 1002106 23:21 /bws
Lab lD: C06O9123&@2
Cllent Sampfe lD: Fitter 4802 conbined with Beaker 25Matrix: Fllter
Colloctlon Date: 09/15O5
DabReceived: 09/26O0
MCUAnafsesResult Units eustifier RL eCL Me$od Anotpis mrBy
RADIOiIUCUDES -TOTAL
Uranium, Activity 1300 pCilFitter O.2 SVm020 fin2rc6z3:2'ttus
Report RL -Anatytg raporthg limit.Deflnlsons: aCL - euality control uhil.
MCL - ltlaximum conlaminant le,veL
ND - l.lot delcded at the nportirg Imil
APPENDIX D
Figure 1. Facility Schematic Representation
Scrubber Process Data
D
Inte rtnati onal lJraniumFacility:
Stack rdentin"u,lon, North Yellow Cake Scrubber
cu Distance upstream from next disturbance, feet
Distance downstream from last distubance. feet
y: Distance of Sample Level to floor, feet
O: Stack Inside Diameter. inches
Estimated Moisture, percent
Estimated Temperature, oF
Estimated Velocity, frm
Number of Ports
9.5'
B:9.5',
65'
19"
Near Saturation
70-125
1.100
l+a+l
Control Unit
Type:
Figure l. Facility Schematic Representation
:Q'h.t'c-L't
6ei o'hohah
o'h
o'h
o't-,
Q'hohol"
Ug
bs
b's
=lofS{7
-7f"-S
ot',ll
gv: o\
t'ltct
00".Q I
b?'. b
4o' p
qhrYz
;
41 7./---\
@)
WrL
90"9
lhir.,
L\,"-L
-$h:l
0'1" | 1
a1g:-Ll
@
9t, :ll
Ql:t1
4h "ot\1,'.ol
ss .b
o€.b
Lo "bth *on:,J
u'ho's
)e
o'Q
t's
a's
l's
8'e
L'g
b'L
4'€4c
b'c
a'h
L'L
L- t-
L'Lq'L
t.aIY
ls
l's
x.9
e'9z'9
z'st's
,.rOg ry) .tc f n
i.llntr; Y(W
---:
0)'L
4,'L
0'ut)'L
/) t-
1't'q'L
L'L
L'L
L.L
L't&'r
9=^ t-
9' t-
lrL\J?t{Q qd J4rn1
oTf"tcS v'.tl4J
ttsqn'u,e -J,q 22 *lPly Y+tW
APPENDIX E
Calibration ofthe console dry gas meter(s), pitot tubes, nozzles diameters, and temperature
sensors were carried out in accordance with the procedures outlined in the Quality AssuranceHandbook. The appropriate calibration data are presented in the following pages. The nozzle
calibrations are recorded on the first page of the field data sheets.
Figure 2. Schematic of Method 5/ll4 Sampling Train
Meter Box Calibration Data and Calculations Forms
Post-test Dry Gas Meter Calibration Data Forms
Tlpe S Pitot Tube Inspection Data
Sample Box Temperature Sensor Calibration
E
Iirrpcrs!-rt$1 FDbYl:dilffiJ
-il tjDo I
FUTlbo
.i
, ''''.: -
Irqinpf Train gptionel; IrhV * Replaced
. EyAl tsqu\E ont corrcbrsdr
I'I 'l
IlTI
I
I'.t.t
'ruger/l,(
-^-.--\ I
/lTypes{r,r,o. \
Shck
uruGoosened<
l,h?do
\\
FbstTracod
Casslited
Probe
\CtEck
Enaty sfica
C€l
Ar-Tght
|,trrp
Ivhmrnrter
', A
I
I
Gtass Fiilter
l-bkbf
l'b*dArea tlirll
iii i 'ln, liil Iri
lit
TI
I
I
I
I
-J
lirr YyuEr llll
tlll B'* ililtU ilt
FIGURE L .SCHEI,IATIC RBPRESENTATION O, fu OO4t1r 'nl,rNc TRAIN
METHOD 5 DRY GAS METER CALIBMTION USING CRIT'CAL ORIFICES
1)
2l
3)
4',
DATE:
METER PARTIT
serect three citcar ormces to oaribrate the dry ga' meter which braoket the expec-ted operating range.Recod barometric pressure before anO "n", orflOratton pro""Orr"l'Run at tested \€c!um (from O.dfic€ Calibraflon R€port), ti" p.i*
"Orn"necessary to achla/e a minimum total \olume of S oubic fBet.Record data and infomaflon tn the GREEN osil", Vi[Oil c"ff.
"re cabutated.Facility
FINALl, tl
AVO (PL)
25.39
MEIER SERIAL f
CRITICAL ORIFICE SET SERIAL *
',,;irr" j
Jlois*'.' gir**, i
grs,!$e,'
BAROMETRIC
EqUIPMENT ID *IF Y VARTATION EXCEEDS 2.OO%,
ORIFICE SHOULD BE RECALTBRATED
I
t
ffi:ffiHrffiH:ffi
vqr*, = *,tPbq +@
^lTottb
r =v!l:c-Vm<at
0.997
g+*
:0.S94
jo,ge!
1.91
l.00ri
t4q
+sF
t4t1
f;007
tr999
roos
:lzn7i,1
:!,O70ll::
r!,?99i1
:l.o*r;r,
:lcio I
tzos,':l
ii#fl
,C{9s
4{707
:::::i{+#
fiapl
.4.3qt5
r1t€E,
i€s
$rge
,!{tr!r ,
qie963
.441,31 :, .
AVO r
1#l
f49,. r
4:rFs3 .
AVG:
4:2?ai
4.s252,,,
4.i2qtr '
AVG.
.fr:63
.o.04
s€g
.1.76
1#
i.rs
:]|,
1.66
lEg'
l;d5'
1.9
1S
1.VUSING THE CR]TICALORIFICES AS CAUERATON SIANOARDS:
Ths fdo$ing equsrom io us€d b cdcrrare.he eunao vcuma ot * pas6€d urough he oGM, vn (8t0, and ho cfirhd odrhr,vc ('rd), 8nd tho Dcfrr cdbarbn hh, y. Th.uc equahns re auiorurey rer,ra.o m uo sprs&hoot $o's.
vmp,a1 = Kr*yr*Pbar+llH /13,6)
tm
(r)
(2)
(3t
= Nel \olume of ga8 sample passed through DGM, conected to standard condition8Kr = i7.64 h/tn. H! (Engtish), O.385S.I(/mm Hg (Metrtc)
- -' -
T, = Abootut DcM .vg. i.mpcntup CR . English, .K. Mofic)
= volume of gas .ample pa8'ed through the crltloal orlfice, ooffecled to standard condiflohsTd : AbEolute rmbi.nt bmFr.tur. fR . Engtirh, oX . Mctic)K = A\€rag. K, hstor fiom Crttcal Odficc Cslib||tone OGM calibration hc'tor
ELAPSED
TrME (MtNl
offi*j: :ffiffiffi**ffiffi
x, ffiffi?4,q : [,.,,is!oi l I 0,$,
AvERAGE DRy eAs METER cALTBRATT.N FAcroR,
" " [@l
AVEMGEAHq=lETl
or'= (ffi,)'^"(ry)
Console #3 Callbrauon
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFIGES
DATE:
METER PART *:
1) sslecl thrc€ critical orific€s to calibrate the dry gas met€r whlch bracket the oxp€ctcd operating rangc,2) Record barom€tric pre$ure bafor€ and aftsr calibretion procoduB.
3) Run at t$tad vacuum (tKrm Oriticc Calibration Rcport), for a pcriod of tima
necr3sary to achlcve r minimum total voluma of S cublc fgot.
4) Rccord data and information in thc GREEN cr[s, yELLow cels are carcuratad.
BAROIIIETRIC PRESSURE
EQUIPIIENT ID *:
Il,.',q ffil
AVG (Pbl
25,35
ITl ' fmlFii
l, ,r, | ,trir...Tj.Fl
I , ,.1 r lo.Coool'-rs Iffiiffiffiiffi i|i i:liriir;!iritr:u::rl
:it!t
USING THE CRITICAL ORIFICES A3 CALIBRANON STANDARDS:
Thc following cquauons arc uced to calculetc thc atendsrd volumcs of air pars€d through th€ DGM, vh(8td)' and lh. critlcal oriflco, Ve (std), lnd th. DGM calibration faclor, Y. Thcsq cquailonc arc automatic€ly
vm,.,^ = 1g, * y^. Pbar + (N! | 13'6),TM
vq,--, = y'* Pbar * @
JTamb
. .ltiirol'
: , ,, I :'l : : : : i i : : ! I I i I I , : i i. . : :
i:,iii{!ti{f$ri
6,0115
6.032
5.030
tF Y VAR|AT|ON EXCEEDS 2.OO%,
ORIFICE SHOULD BE RECALIBRATEO
1,011
1.010
1.O14
AVG r 1.012 0,00
AVG 3
AVG.
1.6it
1.63
1.62
.0
,0
,0
,0
.0
.o
(1)
(21
., Vcrr,^I=-Y^ut,
FaCility lnternational Uranlum.North yellowcaks Dryer Scrubber
79,76
81.5
t!
0.00
0.00
0,00
0.00
0.00
0,00
' Nst vorumc of gas Eampr. pass6d through oGM, conected to standard conditiong
K! . i7.64.Mn. Hg (Engtirh), O.3sS8 olvm Hg (M€rrtc)
Tn = Abgolut. DGM evg. temperstur. (oR - EnglBh, oK _ Met ic)
' volum€ ot gas sample pabsed through the critical orifice, corrected to standard conditiongT6 : Ab$luto mbisnt t6mp.€turc fR - Engtbh,.K . Mot ic)
K = Avoragc K tactor from Criilcal Ormca Cslibrsti;n
ELAPSED
Tn E (UtN)
e
j,ii,,...i1;,.:l' ,j;,''::itt!l
;rZa,l,i;';;,t[ :];;;:tttl
i;,,'lz ,: rii ,,1 :-,:ro ,iii3l:i
Hp| 4.20s8 4'2s12
"l | 4.rsr4 4.22lg
I e.Pq I l 136,, l 4.1sz' 4.2ose
FfrffiIiltrIffiffiIT]E-
AVERAGE DRy cAs MEIER cALtBRAIoN FAcroR, ,. lffil
AVERAGEAHo.I 1.63 |
*." (ffi)'*(Y)
i, ilij1;:[;i1,il;;iii
.;:: ; l:;1;i1.1; ,,r ; .1.
I l: : r : ir ! i i: :i I l '",
'' ' ,.l,,; ..::.
ai,, i:iiii;i:i; ii;il ilriiiri i:li iiliilii!:il::l
dtrffi iilt: rlll
i:Iiilt'iiti:lliti
r : ! i i: I : : I I : i I I i i: I i i I :
ir;iiiirIi t::t:tr:!
(3)! DGM calibratlon tactot
Consol€ #3 Calibratlon
o'g,' t:z/-? i" (
Type S Pitot Tube Inspectiolr Dgta
: .: pitotTubcldeatification: 21- Z
q=.2)T ;n.
P1: 3.fT in
Ps= .)fO in.
PB
Is Pe:Pa ? J
Is 1.05.q < q < 1.50 .Dr?---=-
c'1<10" o,=l J o
P^
cr2 < l0o
9rS5o Pr=
g
9r<5o
Zs0.125 in.. O)Ain.
w<0.03t25 in. W= .0 L3 in
Thc pitot tube mects the qpccificatiors for a catibrAioo factor of 0.&4? J
ou: 2- o
o- | oP2- |
z=
'Tcmriraturc Scosor Calibration
Type S Pitot Tube Inspection Data
D,= ,7lr in.
g
o,=l'
Ar=l'
,'\Fz=
<---.-_-:- z
z= .O33 . i".
N6 in.w=
Thcpitottubcmcersthespecilicatiorn foracalibrarioa tbctorof0.E4? V/
e^= ,! 4l ;n.
Ps= ''l1l
Is pa=ps? V
Is 1.05. D, < q < 1.50 ,qZ--T
C1 < l0o ct=' .O
o2 < l0o
ip,s5'
F:<5o
ZsO.l25m.
W<0.03125 in-
:J pu
Sample Box Temperature Sensor Calibration
Datc: l]-3a-afiatibriloc 4 tr//"/r.n *"rr*;Z;
UnitID Temperature
Difference
CF)
/
F
APPENDIX F
The testing protocol and other correspondence related to the tests are included here.
QUARTERLY EMISSION TESTING PROTOCOL
FOR RADIONUCLIDE PARTICULATE MATTER AT
TNTERNATIONAL I'RANIUM (USA) CORPORATION
BLANDING, UTAH
YELLOW CAKE NORTII DRYER SCRUBBER
August 30' 2006
Project Organization and Responsibilitv
The following personnel and the testing contractor are presently anticipated to be
involved in the testing program. The Utah Deparfrnent of Environmental Quality, Division of
Air Quality (DAQ) and EPA may have their own personnel to observe all phases including the
process.
Company Contacts
lnternational Uranium (USA) Corporation Wally Brice 435-678-2221
P.O. Box 809
Blanding, Utah 84511
TETCO Dean Kitchen 801-768-0973
90 East Main Paul R. Kitchen
Lehi, Utah 84043
Facility and Location
lnternational Uranium's White Mesa Mill is located 6 miles south of Blanding, Utah on
Higlrway 191. The Mill processes uranium ore. There are two yellow cake dryers with
individual scrubbers but only the Yellow Cake North Dryer is currently in operation and will be
tested.
Test Objective
This test will be conducted to measure the radionucleide emissions on the scrubber that
serves the Yellow Cake ore processing operation at the facility. Testing procedures will include
accumulating process and production data as well as testing for Radionucleide emissions using
EPA Method5/114.
Test Schedule
Testing will follow this protocol for the third quarter of 2006 and the first and third
quarters of 2007. Testing in the third quarter of 2006 is scheduled for September l3-15, 2006.
Notification of test dates in other quarters will be sent as they are scheduled by the facility.
Site Access
The sample site is located on the building roof and is accessed by stairs and ladders inside
the building.
Potential Hazards
Moving Equipment - Yes
Hot Equipment - Yes
Chemical - Yes
Other - Radioactive
Process Data
All operational and instrumentation data will be made available to DAQ personnel. The
facilitv will run at normal conditions.
Ouali(v Assurance
All testing and analysis in these tests will be conducted according to EPA Methods 5/114.
2.
Reporting
Reporting will be prepared by the testing contractor according to EPA Quality Assurance
Guidelines. A complete copy of raw data and test calculations summary will be included in the
reports. All process and production data will be recorded by lnternational Uranium (USA)
personnel for inspection by DAQ and EPA, if requested.
Test Procedures
Radionuclide emission testing will be conducted on the scrubber exhaust stack according
to EPA Method 5/114. Specific procedures are as follows:
1. The sample locations and the number of sample points will comply with the requirements
of EPA Method 1.
The inside diameter of the Yellow Cake North Dryer Scrubber stack exhaust is l8 inches.
The ports are located 114 inches (6.3 diameters) upstream from the next disturbance and
114 inches (6.3 diameters) downstream from the last disturbance.
EPA Method 2 will be used to determine the gas stream velocity. Type "S" pitot tubes
will be used with a Co factor of 0.84. Dual inclined/vertical manometers with graduations
of 0.01 inches of water will be used. If the flows are below .25 inches of water a more
sensitive manometer will be used. The graduation marks on it are .005 inches of water.
Direction of gas flow will be checked for gas cyclonics prior to testing. If the average
deviation is over 20 degrees, then straightening vanes will be installed or other
arrangements agreeable to DAQ will be made.
Test run time will be at least 60 minutes for each test run.
EPA Method 3 will be used to determine the gas stream dry molecular weight if the
exhaust gas is not ambient. An integrated flue gas sample will be taken from the exhaust
line after the dry gas meter orifice during each test run and analyzed at the completion of
the test with an Orsat to determine the molecular weight of the effluent gas stream. If the
exhaust gas is ambient air then TETCO will use a dry molecular weight of 28.84 lb/lbmol
(20.9 percent C.2, 79.1percent Nr) in all calculations.
EPA Method 4 will be followed to determine the gas stream moisture content.
Probe liners will be 316 stainless steel for all tests.
The glass fiber filters used will meet the requirements of EPA Method 5/114.
aJ.
4.
5.
6.
7.
8. The barometric pressure will be measured with a barometer which is periodically checked
against a mercury barometer. The barometer will be checked prior to testing to assure an
accurate barometric pressure.
9. All current calibration data is submitted with this protocol, except nozzfe calibration
which will be done at the test site. Nozzle calibration witl be included on the first page of
each set of run sheets for each respective test run. Any calibration that is not cunent will
be re-calibrated prior to the test dates.
10. Any necessary preparation and clean-up by the contactor will be performed in the
contactor's sampling trailer or a clean area on International Uranium's property.
Laboratory work and analysis will be completed by the conhactor and Energy
Laboratories as soon as possible after the test project.
11. Verbal results will be reported to Wally Brice of lntemational Uranium (USA). The
written report will follow within 30 days following the completion of the test.
12. If maintenance or operating problems arise during the test, the test may be stopped. This
determination will be made by lntemational Uranium (USA) representatives and
operating personnel in consultation with DAQ representatives
Estimates of Test Parameters
The values below are estimates of the stack flow rates and temperatures. These are
estimates only and are not intended to reflect permitted values.
Velocity fom 1100
Moisture % Near Saturation
Appendix A
Facility Schematics
Yellow Cake North Dryer Scrubber
Faci,i,v: Inte frnati onal Uranlum
Stack rdentiri.u,ion. North Yellow Cake Scrubber
a: Distance upstream from next disturbance, feet
p: Distance downstream from last disturbance, feet
7: Distance of Sample Level to floor, feet
O: Stack Inside Diameter. inches
Estimated Moisture, percent
Estimated Temperature, oF
Estimated Velocity, fum
Number of Ports
9.5'
9.5'
65'
18"
Near Saturation
70-125
1.100
l+a+1
Control Unit
Type:Yellow Cake Processing
t
cl
l,
Figure l. Facility Schematic Representation
Appendix B
!- Calibration Data
METHOD 5 DRY GAS METER CALIBMTION USING CRITICAL ORIFICES
1) selec{ three crnrcar odfices to cailbrEt€ tho dry gas meter which bracket the e,p6cted operatng rang€.2) RGcord barom€tru F€s3u1€ bGfo.e rnd alter aaltbailon prooedut!.3) Run at t€ltsd vrouum (hom Orillcs Callbration Rsport), tor ! pcrlo{, of tlm€naoo8ary to aohl! ! a mlnlmum total \olurn€ d E ouua lb!t,4) Reaord data 8nd Infomsilm In thG oREEN ocrb, yELLc'l/r/ ocile are carcurated.
ffi
ffi
ffi
ffiffiffi
IIETER SERIAL*
CRffiCAL ORIFICE SET SER|/AL f
Facility
FII'IAL
lffi+l AVO (Pbil
25,39SAROI|E Rtc PRESsURE 0n H
EQUIPTIEI{I IO'I IF Y VARIATION EXCEEDS 2.@X.
ORIFICE SHOULD BE RECALIARATEO
t
2
3
I
2
3
I
2
3
USIIIS THE CRTTEALORTEES A8 CruERATION 6TAilDAROS:
Th! ftloiog cq'Jllom rs u..d b cdcd& hc ruxbd vdumi d €l p$sod tmugh ho oclt, v. (8u], dd hc qllcd o.ilc.,
Vc (sts), a|d lhe DGM cdbcton ffir, Y. The Gquaton! ac aubmslcdycdcuabdln h! ryShootdov..
(11 vm,n=Krlvn.Pbar+(ry1\3.6)
ffiffi
Hffi
ffi
:::::,i::::::,i:;:::.: : .:: ...,.::
:,,:ti*lf,f i,, ,,:,, ,149S,1: ,,, ,, ,' jg,gpl,
i,i,g49*l.,.1,,.,,,sAgq::' ., : :, +pi,
t:i:t.liiiI,,i t., +:ingra,,,: ,, ." ;*
AvG - ': :b:-
:.:::i ::ii'i:i::.: :.,,,.::: ::1 ,.T:
:.i11#',:.,.,,. 1#:: , ,i l9P?
:.,Ceg:i : : .4a1pg ., Ig
'l ii,3cbd.. . ...,'t:sss3: . t;ooo
AVO -:r: .lr.| ,',..... .,
!i!.Q$!:l:lr 4123!1;
l: ,:i: .i. ..i ::{€9, , ': 4!s4?': ,
:f4p',1'r , :EE3le
"AVG.
ts'j4i
,r+q
.l;008
i iriod:
r;lllg::i
,, r$Ig:iii
l:.:I:7!:: :
ir:6C.,:t,,
i.::Lsc.ii'I !:66i,::
.... ,:.1:65ii,
@ "1' ,.,,,,,,,
''1.6i , .
, ,l-ct,,
1:el
r Net \rolum€ of gr3 slmpte pes€€d thot€h DGM, con€cted to stlndard oonditons
Kr ' 17.O1wln. tb (pngllth), 0.3SgE 1(/mm Hg (M.dc)f, - Atrotutr DGM 1ry. tompcmUr fR - EnglLh, oK. Mrtic)
. volume d gaa 6amplc passed though th€ crlUcal odflce, ooreoted !o standard condiilonsTd 3 Aholut rmbLntUmfnEn fF. Engtbh,cK. Meic)
K 3 Av.ner K hcbr |toflr Cdtcal Otfic! Crllbntoo
AvERAGE DRycAs METER cALTBRATIoN FAcToR,"=@l
AvErtAcE alto =lrerfll
o""" (uffi,)'*(ry)
(z',)velat = K\Pfe#
Y =V:*.lmtal
(3t r OGM oallbratlon lbctor
Comole #3 Callbrailon
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Scr€d thrG6 qiucar ori'cca to c€ribfatr th€ dry g". mc!.r s'hidl brack.t th. oxpcc{ld opcratng rang€.2) R.co.d b.rom€tlc pna.turrr bldor. .nd eltcr celtbraifon xocoduc.3) Run .t tartcd vrcuum (trom Orlltc. Callbra[on Rcport), ior e porlod of tmcnco!.rary b .chh. a mlnlmum lohl volum. d E qJbb,.ai.4) R@rd dat and Inform.Uon In Ot. CREEX c.L, yELLOW cclr rn c.tcutrt d.
, TETERSERIAL
CR|NCAI ORIFICE SET SER|AI
INIIUL
*o*rr*" ,*rurr*a un "or,lllrlEQUIPIENTID|: I Conrotrtt I
IF Y VARAIION EXCEEDS 2.0096
ORIFICE SHOULD BE RECALTBRATED
RMI.| *rl AVG IP|')
26.42
l-ll ' l-."" 1L"J:m+Ft;l;m| | .l;T;ll-;lrffi| | . l.rr.rT;i
t.175
a00t
5,20a
arG3
9.11i2
6.16t
,.14
E,1U
t l23
USING IHE CRffiCAl OR|FICES AS CAUBRATTOI STAilDARDST
rhe lblordng equatons E|r us€d b cdorbh bo shrdard rtums ot rlr psss€d b|!Wh t\O DGM, v. (s6), aflr $6 glftd
orillca, Vo (sts), a|{ be DGtt catbraton f&r, y. llreco equa0one ao &b|nalcaly cahjabd h Ue lpo*he€t above.
vmsa., = K,' y^. llgffJ 13-'6)
vc1"at= *"'o{'?\lICtnD
TI:28
f6.
76
7aco
76.76.
76.16
76.60
74.00
fa.25
1'119!
LW.
4.3360
AVGr
0.96E
lxsl
0.984
90!
g,cz
1.49
1d0
1.49
Llt
l.5a
1.il
1.Q
L€
1,8
Silt.l0i ct:t 7at
ttiLTSl 8tt.e0!
Ett.co3 tc+ota
t6a"o6ao 8C3.iar
aaa.t9t c7+ti22
E7132il 87e,,46
l-,;l| ''.t. It;IEg
| 0..2 |
l---;l
Eil
HI rr.zc I
{5931 4.5709
a!320t 1-2979
,,!!oz ..2e6o
4.3210
4.3112
43084
Avc. 9.991
{,3184 0.999
4.3079 0.999
l.lotc a.99SAvcE g.9gg
0.e86 LZ:
0.995
9€9t
b.eeo
0!
(2)
r Nrt voluma Ef gas rample pa$cd through DGM, coar€cled b standard conditongtq . i7,Af htn. H9 (Engil$), O.3E5E.K,ryr He 0&rdc)
T. , Ab.old. DGM ryg. tmp.n0n (h _ Eneil.h, k - Mtt|c)
' volumc of gas rampto peatrd through thc crldcal ortf,ca, comc,tad to at ndrrd condiuonrTd i Ab.oln rnbbnt rfr|psll.r (t - E ,ghr,. a - M.!b)
K g AVJICE Kt ctrfon Cilfc.t Orlfic. Ceilb..ton
Y =v"u',v^r^
OutoF
32
63
116
32
g2ri
ENVIRONMENTAL SUPPLY COMPANY
8:lz83a ulg.00t
t3amr qal0{
taS.l0a tat 30t
It 71 7a 7t 83
3e 71 tt 71 n
ct 73 7:t 7E EO
f-lts I l__aql ..3700
l-r* ll.r"l ..!212
| ..ao ll2.trl 1.&u
cg ,t 71 79 lo
tt 7a 7a 77 t0
70 73 71 70 8t
70 71 f5 7i 7a
70 7a 7a 7E 7l
f1 7t 7t n 7A
AVERAcE oRY GAs TTETER cALrBRArtoN FAcroR, y : l-6t-l
AVERAGE aHn =l-T3dt-l
AHqr 1 o.rse'lt ax /y^tgg[\vJerd)/ \ v- /
Tampcnfura Sonro]!Rcfomnca lnOF OF(3). DGM c.llbnilon f.clor
32
63
119
Console {14 Calibratlon
(
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Sel€c-t
'hra€
cdticel orflicar io ceribratc thr dry g' mctcr whrcfi br.ck i rh. .r*€cr.cr opcrarng rangr.2) Rccord b.romcfic prltluo b.,lbr. .nc mrr jiunuon pJr-,3) Run .t torlrd vrcuum (trom Ortfto. C.fibntm R.pon), iii" ai* , orn.noco$ery b .chl.vc a mlnlmum btal rolumc ol S orblc fcct.4) Rc€rd dalE and Iniormeuon ln th. GREET{ calr, YELLOW c.I! rr. cltcuLtrd.
DATE:
UETER PARTT:
IETER SERI{. I:
CRlTlcEL OruNCE SET SEruAL r:
2tt-all 296.ala
29t alt tOtJfiIO
loL20 totaz
amlt/3ta.E8t
31a,tt!lla.Slt
319.tcl s2atE
t2t3tm 33o.3t1
rito.t71 335,37a
33t 37a IrlO.SEl!
AAROTETRTC PRESIIURE (tn H
EQUIPIIENT ID T:
at at t3 ff 7A
Ct a v 7e 79
tt u It 7t to
at tt g,7'8l
at a,89 tt a2
tt ta ,o tl t2
FNAI_t*"1 AVG (Pb)
25,t7 IF Y VARIATION EXCEEDS 2.OO!T,
ORIFICE SHOULD BE RECruARATED
l.|,|rt
o.eeq
0.99.1
E'ffi[;l:mFI I, ['-'T;-l
l-;lrffiF| | .l.'..T;.l
vrlut= *""u{'P
al IAmD
Y =Y",,*,v^u*
t ooa
t.001
t.002
t.act
!.00a
t 00Go
a00l
5,003
r,000
71.7t
00.7t
82
It.00
t{.7t
E6,2t
86.25
86.76
IEJt
/r.t'180
L1253
1.1Ut
rlJll!
/tlOt8
4.0951
Leo
4.O2
tsl
i.63
rd3
l,el
t!1
l,!1
1,42
lJ3
l,tt
'Avs. 0.Sg!
4.5885 t.o.tl
..175't 1,011
,l.ltl6 !4CZ
AVG - l.oto
..r.te8 lJ92
aJ,M l.oo2
5J2'4 t99IAvcr lJ0!
4.!I
USll{O nE CTTICAL ORTRCES Ag CALlgRA.not gtAlD nDgi
The brorin cque0.n. a,r us.d b c.rcurar, t F stsrdsd rcrfirr of et g$s€d tru|gh u|o DGlr, v, (ru), gd ho crlfcdodflor, V. (s6), and he DGM c$.atDn facbr, y, Ihola oqusfms r'r arbmEfE ly cah,lsbd fn Ura spnedd,sot abovo.
Yilu't = K, * yn, Pfor + l4!l 113'6)(rl
l2l
! Net vorum€ of gar sempt pasrad thrcugh DGM, cofilcbd to standard condi0ons' K, . f 7.A{ hIn. }tg (Eneild,), O.3S5S lgu,rn Hg (Mrf|c}
. T, r Abrold. DeM .v9. trnp.rdw (h - Englth. 1< - M.t tc)
t volumc of g.r 3empb pa!3ad thEugh lh. oducsl orilic!, comciod to shndard condltonrTd I AbFtut ..nbt nt t.|ryrrrtn fn - ern[$, 1< - f,b!lc]
K r Ayrngp K Edorfiqn Cd0cal Ortic. Csllbnuon
aH" ('ffi,)"*(ry)
Tampcrtture SansoERdcrrncc lnToF OutoF
31
T7
111
31
75
111
30
77
1t3
[.MAL
at l9 at 80 8t
0t c0 02 80 8t
0t a2 ot 12 E'
+- | + z!o_-l 4.rs6i 4.187s
t_ zlo | +rzrtr ,.1!t!
I .,.r | | aEo | fi$! ..142aEEffiEfr|''-l t-;t
HH H#
AVERAGE DRYGAS iIETER CAUARATIOTI FAGTOR, Y T I_1.OOr|
Ar/ERAGEAHo=fTEiS-.l
(3). DGM c.llbraton faclor
Console ll5 Calibration
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1)
?',)
3)
4'
seloct rhree crilicsr orifices ro c€ribrato tho dry gas mot€r whroh bracket the exp.cted operaling range.Record barometric prcsure boforo and afier cellbrelion procedure,
Flun at te€led v€cuum (from Orlfice Catibrailon Report), ior a perlod of limenecossery to echiove a mlnimum total volumo of S oublc feol.Record data snd Informailon in the GREEN c€[e, yELLOW cers sre oarouraled.
METER SERIAL *
CRITICAT ORIFICE SET SERIAL
'A
BAhOMETRIC
EqUIPIENT ID *
FINALl"iil AVO (Pbrl
25.70 IF Y VARIATION EXCEEDS 2.OO%.
ORIFICE SHOULD BE RECALTARATED
ffi
ffi
ffi
;t:sgg*i
::: {sl6t::
I..a3092:!
ii#l+..
,:X#,,lg:sdzc,'
.l:S,?0?i , : lr;0o3
.{#ii.,..l.,.'.'.: lil{12 ::.: : : I . ' ', : :,t:007
ffirffiil
[..=lE#l
Hffil:::::0re :'l
.42;45!l
l+ll.asili
AVG r i,oii7
r;i:r.::,:
'l:001:
-:0.999,'
:1-005 i:
oAa :
,{1.{:t,
' AVGg . r:::i602
_::,::t.,:i :: t:::.:::::i .:: _.: :-,,;!g':, W , 'slez
'4:2P :fAXs' "o.isr
,:44pir, , ll!e{ , tssl
AvG ' o'ii8
,$.0?l
(11
(2',t
u
66
120
Out
oF
u
66
120
ENVIRONMENTAL SUPPLY COMPANY
ffiHtfrlillffilffit { i,,,i.il
l :ogrit::t ir' 'l
ffi. ii*trilr ffiiiffil ffiffi
ffilil'*fr* ffiri'$fii'i ffi:,,90.If
r,, biloe
r:ir1i75
::::,.:::t:i
il:!l!i-oo
irr r'diiie
vm,-.^ = K, "vm'PbE+(NI /13'6)
IM
vs<,a>= *'t'u3-'tP
^t I cmb
f =v"roo'Ymod,
1
2
3
1
2
3
USING THE CRITICAL ORTFICES AS CALIBRATION STANDARDS:
The fobwing equatiNs eg usod to c€buHs tirre stildrd rclrFs ol tir passed h]u:gh ua DGtvl, v. (sld), rd t|e critbalo.ifio6,vo (std), ''d the oGM cslbralbn f*tor, y. Th6ss squstbns sB anomaticaly csbubled in fu spr.ad$Fat sbcryo.
E Net volume of gas sample passed through DGM, con€cted lo slandard conditions
K, = 17.64 "R/in. H9 Gngtish), O.gS58 1(rmm Hg (Uetdc)
T. = Absotute DGM a\tr. tEmpersture CR - Engtish, oK _ M6t ic)
r volums of gas sample pass€d through tha cdilcal orttice, correc,ted to slandard condilionsTo = Absolub ambient tomperatun fR - Engilsh, oK - Metic)
K = Awrage K factor trom Cdtcal Orifics Catibration
AVERAGE DRy GAs ME'ER .ALTBRAT.N FACroR, y = |rildfrtl
AVEMGEAH"=
AHj= ( o.zoe 1'? aH /V_l$l)\v.,{std)/, \ v- /
Temperature SensorsRetcrence lnOF oF
33
67
121
(3)= DGM callbrallon facior
Console 116 Calibration
Type S Pitot Tube Inspection Data
-
: .: PilotTitbc ldafincation: Z7,;^"r*,.0,-rOIW\t .l
4= -Z5o in.
P^= 53? io.
Is Pe:Ps ? ;tIsl.05.qSq<l.50.Drt y' '
tt1'< l0o ot =' -t
Yr- =j4 in.
z
Fr=
z= .Ql D n.
g
W30.03125 in.w: - oo3 tn.
The pitot tubc meets lhe specifications for a calibration factor of0.g4?
cr2 < l0o
: 0rS5o
z
I
#z
P2<5"9z=
Z<O.l25ir..
.: .PitotTirbcldcntification: 21 - Z
-ra'h .LJwirL--....:...:
P1= 3 .tro in
Pg= .)f,O iD.
. Is Pa=Pe?
Is 1.05.Q< q< l.50.Dt?
c1'< l0o
a2 < l0o
9rS5o
c1 =' J 'o
/
H-
W3 0.03125 ilr.w= .oL3 n
Thc pitor tubc mccf.thc spccifcatiors for a catibratioo frctor of 0.g4? J _
2_o
'Fr=Oo
l
Fr<5o
z
230.125ir..
R-r
z=-- 'o)(in'
Ypz
Type S PitotTube&rspectiofr Data
i : Pitot Tubc ldcntification: f,-7 - 6
'rc*niciaa: K.a -{^-, Gort
q= , J7r in.
c-r=l''8:
loDr - I
Fr- O, '
m.
$i/= db
'Thc pitot. tube mcefs thc gpccifications for a calibrarion faao r of O.UI /
n^= ,!4[ n
Pa = '.'14 |
Is Pa=Ps ?
Is 1.05 : D, < D, < l-50 ,Dr? r/
d1 < tOo dr=' .O o
,at 1 l0o
''.i Fr35o
.Fr < 5e
z:.o33
-€,",
H-
crl<ld
c2 < I0o
A 2aoPI -.J
I
a 2ao
Ws0.03l5iD. ."'' W=
The pitot tubc mccts thc st*cificatiou for a crlibrarion fraor of 0.t4?
. >(-\DrE 7u u in.
ra- JS-e/ in.
. p"= ]f4. ;r,.
Is P^=P"7' ,/
Is I.05.4 S D, S l:50.4 ?--
-
orE' '.2 'o
.t o
R:- 2 . ola_-
;.
0
Datc:q lZ-z? -or
Q (rv
I
Dr=- Z Sn h.
Ps=
Is P^=P"7' t/t.os'q<Dr3r,so.qrl
ra- 3 f,y' in
3r-q i"
l*ar=' I '
g o,'tO'
o1 < l0'
,,' ._, FrSf
F: i5o
si=
w= .4t2 in
\lo
j F;
1-Z
Zs0.125in.
W 3 O03125 iD.
Thgpitottubcmcctsthcspocifrcrtiors foracalibration facforofil.8 4? r./
Refcrcnce:
Datc:q tz-?-z -oS-
g
; .
'rirotruu"td*tifi..rioo: ld- E
I
I
\
c; < l0o
t Fl35o
Frtf
Zs0.l2Sin
|.
Ws0.03125io. " fu=
Thc pitot tubc mcets thc spccifications for a crribntion factor of0.g4?
0r=
g; .l o
z; .O O'l i-
i
m.
D,= ,37t i,.
e"= .1177
ea- .</.27 tn.
lIL
. Is Pe=pa ? VJIs I.05.qS D,< t.50..D.? {
'or=-. './ 'o
ar=Oo
al o.. v
Sarple Box Temperature Sensor Calibration
I
\
l
\
r Oomplote iterm 1, 2, and3, Also complete
it6m 4 fi ResHcted Deltvery is deslr€d..r Prfntyou,r na4e and addrcss on the rwersd
;so tha! wB. can r€tm the candto you,r Atactr thts card to tbe back of tho mdlpleL€,
orontro tontf sPace Perrn'tts.
l. ArtHeAddassed to:
tr Ag€nt
C. Dato of t)61tu€ry
gt tr Yes
,8, Ho
Elnwrca l Eo.o.o.
4. R€sfrfcisdD€lh,€ty? @ta Fa)EYes
7;4t*J Spatt
ul--h b*Q
PrD . tsoX tlttlSzo
4"t t tKc G(y W
^f.iltt4 - 482o
\
I
3".S€rvlc6Typo
Fc€fiifl6d Mall tr EarssMall
E negntersO tl Rettnh€c€lptforMdtrttar.tdho
-2. Ardch l{trl$€t
sa 0bo.@€,
Ps Fonn '1., Febrr,rary 9on€sdoR€tm.R€peFt 102595'o2-DFlerc |
?00,*-ff 5E- noo:,-zzu10oas? I
I