DRC-2005-001106 - 0901a0688080578e

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National Emission standards for Hazardous Air Pollutants
2005 Radon Flux Measurement Program
White Mesa Millsite
6425 South Highway 191
Blanding, Utah 84511
Prepared for:International Uranium (USA) Corporation
6425 S. Highway 191
P.O. Box 809
Blanding, Utah 84511
Tellco Environmental
P.O. Box 3987
Grand Junction, Colorado 81502
Prepared by:
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TABLE OF CONTENTS
PageI.INTRODUCTION ......... 1
2. SrTIr HTSTORY AND DESCRIPTION .............. I
3. RECIULATORY REQUIREMENTS FOR THE SITE........... ....,.........,.... 1
4. SAMPLTNG METHODOLOGY..... ....................2
5. FIEI.D OPERATIONS............. ........2
5.1 Equipment Preparation.............. .............2
5.2 Sample Locations,Identification, and Placement.. .....................3
5.3 Sample Retrieval ................3
5.4 Environmental Conditions........... .........3
6. SAMPLE ANALYSTS ......................4
6.1 Apparatus............... .............4
6.2 Sample Inspection and Documentation ....................4
6.3 Background and Sample Counting ........4
7. QUALTTY CONTROL (QC) AND DATA VALrDATrON............. ........ s
7.1 Sensitivity.............. ............. 5
7.2 Precision................. ............. 5
7.3 Accuracy........."...... ............. 5
7.4 Completeness ..............."......6
8. CAT,CULATIONS .........6
9. RESULTS ................ .........................7
9.1 Mean Radon F1ux............ .......................7
9.2 Site Results ......................... 8
Appendix A. Charcoal Canister Analyses Support Documents
Appendix B. Recount Data Analyses
Appendix C. Radon Flux Sample Laboratory Data, Including Blanks
Appendix D. Sample Locations Map (Figure 2)
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1. INTRODUCTION
During .Iune 2005, Tellco Environmental, LLC (Tellco) of Grand Junction, Colorado, provided
support to lntemational Uranium (USA) Corporation @C) regarding the required National Emission
Standards for Hazardous Air Pollutants (NESHAPs) Radon Flux Measurements. These measurements
are required of IUC to show compliance with Federal Regulations. The standard is not an average per
facility, but is an average per radon source.
Tellco was contracted to provide radon canisters, equipment, and canister placement personnel as well
as lab analysis of samples for calendar year 2005. IUC personnel provided support for loading and
unloading charcoal from the canisters. This report addresses the procedures employed by IUC and
Tellco to obtain the results presented in Section 9'0 of this report.
SITB DESCRIPTION
The White Mesa Millsite facility is located in San Juan County in southeastern Utah, a few miles
south of Blanding, Utah. The mill began operations in 1980 for the purpose of extracting uranium and
vanadium from feed stocks. Processing effluents from the operation are deposited in four "lined"
cells, which vary in depth. Cells 1 and 4 are used solely for "liquor" storage, while Cells 2 and 3 are
used for sand tailings/liquor deposition.
Cell1has a total area of approximately 270,624 square meters 1m'1. ffris cell was comprised of fwo
sonrce regions that requir#NESHAP; radon monitoring: approximately 267,604m2 of the cell had a
soil coveiof varying thickness, and approximately 3,020m2 of exposed tailings "beaches". There was
no significant standing liquid in "low" elevation areas within Cell2.
Cell 3 has a total area of 288,858 rn'. Thir cell was comprised of two source regions that required
NESHAPs radon monitoring: approximately 156,452 m2 of the cell had a soil cover of varying
thickness, and approximately 28,388 m2 of exposed tailings "beaches". The remaining approximately
104,018 m'was covered by standing liquid in "low" elevation areas.
Due to worker health and safety concems expressed byboth IUC site personnel and Tellco monitoring
staff, a portion of the areas of the wet beaches and covered areas of Cell 3 were not sampled due to the
extreme instability of wet tailings beaches and soils.
3. REGULATORY REQIIIREMENTS F'OR THE SITE
Radon emissions from uranium mill tailings piles are regulated by the Nuclear Regulatory
Commission (NRC) under generally applicable standards set by the Environmental Protection Agency
(EPA) for Operating Mills. Applicable regulations are specified in 40 CFR Part 61, Subpart W,
National Emission Standards for Radon Emissions from Operating Mill Tailings, with technical
procedures in Appendix B. At present, there are no Subpart T uranium mill tailings at this site. These
regulations are a subset of the National Emission Standards for Hazardous Air Pollutants (NESHAPs).
According to subsection 61.252 Standard, (a) radon-222 emissions to ambient air from an existing
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uranium mill tailings pile shall not exceed an average of 20 picoCuries per square meter per second
(pCi/m2-s) for each pile or region. Subsection 61.253, Determining Compliance, states that:
"Compliance with the emission standard in this subpart shal1 be determined annually through the use
of Method 115 of Appendix B."
4. SAMPLING METIIODOLOGY
Radon emissions were measured using Large Area Activated Charcoal Canisters (LAACCs) in
conformance with 40 CFR, Part 61, Appendix B, Method 115, Restrictions to Radon Fhx
Measurements, (EPA, 2001). These are passive gas adsorption sampling devices used to determine
the flux rate of radon-222 gas from a surface. The LAACCs were constructed using a 1O-inch
diameter PVC end cap containing a bed of 180 grams of activated, granular charcoal. The prepared
charcoal was placed in the LAACCs on a support grid on top of a 1/z inch thick layer of foam and
secured with a retaining ring under 1% inches of foam (see Figrre 1, page 10).
The sampling effort commenced on June 6,2005. One hundred collectors were placed in each region.
Due to worker health and safety concems, measurement of the wet beach areas was limited to areas
readily accessible by foot near the toe of the soil cover. Each charged collector was placed directly
onto the surface (open face down) and exposed to the surfac e for 24 hours. Radon gas adsorbed onto
the charcoal and the subsequent radioactive decay ofthe enkained radon resulted in radioactive lead-
214 and bismuth-2l4. These radon progeny isotopes emit characteristic gamma photons that can be
detected through gamma spectroscopy. The original total activity of the adsorbed radon was
calculated from these gamma ray measurements using calibration factors derived from cross-
calibration of standard sources containing known total activities of radium-226 with geometry
identical to the counted samples and from the principles of radioactive decay.
After 24 hours, the exposed charcoal was transferred to a sealed plastic sample container (to prevent
radon loss and further exposure during transport), identified and labeled, and transported to the Tellco
laboratory in Grand Junction, Colorado for analysis. Upon completion of on-site activities, the field
equipment was alpha- and beta-gamma scanned for possible contamination resulting from fieldwork
activities. Al1 field equipment was surveyed by IUC Radiation Safety personnel and released for
unrestricted use. Tellco personnel maintained custody of the samples from collection through analysis.
F'IELD OPERATIONS
5.1 Equipment PreParation
All charcoal was dried at 110oC before use in the fleld. Unused charcoal and recycled charcoal were
treated the same. 180-gram aliquots of dried charcoal were weighed and placed in sample containers.
Proper balance operation was verified daily by checking a standard weight. The balance readout
agreed with the known standard weight to within r 0.1 percent. (Appendix A).
After acceptable balance check, empty containers were individually placed on the balance and the
scale was re-zeroed with the container on the balance. Unexposed and dried charcoal was carefully
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added to the container until the readout registered 180 grams. The lid was immediately placed on the
container and sealed with plastic tape. The balance was checked for readout drift between readings.
Sealed containers with unexposed charcoal were placed individually in the shielded counting well,
with the bottom of the container centered over the detector. The background count rate was
documented on the radon flux measurements data sheets. Three five-minute background counts were
conducted on ten percent of the containers, selected at random to represent the "batch". If the
background counts were too high to achieve an acceptable lower limit of detection (LLD), the entire
charcoal batch was labeled non-conforming and recycled through the heating/drying process.
5.2 Sample Locationsr ldentification, and Placement
Designated sample point locations were established within each region. A sample identification
number (ID) was assigned to every sample point, using a sequential alphanumeric system indicating
the charcoal batch and physical location within the region (e.g., A0l....4100). This ID was written on
an adhesive label and affixed to the top of the collector. The sample ID, date, and time of placement
were recorded on the radon flux measurements data sheets for the set of one hundred measurements.
The sampling locations were spread out as evenly as feasible throughout each region. Prior to placing
a collector at each sample location, the retaining ring, screen, and foam pad of each collector were
removed to expose the charcoal support Sld. A pre-measwed charcoal charge was selected from a
batch, opened and distributed evenly across the support grid. The collector was then reassembled and
placed face down on the surface at each sampling location. Care was exercised not to push the device
into the soil surface. The collector rim was "sealed" to the surface using a berm of local borrow
material.
Five collectors (blanks) for each region were similarly processed and kept inside an airtight plastic
bag in the collector during each 24-hour testing period.
5.3 Sample Retrieval
At the end of the 24-hour testing period, all collectors were disassembled and each sample was
individually poured through a funnel into a container. Identification numbers were transferred to the
appropriate container, which was sealed and placed in a box for hansport. Retrieval date and time
were recorded on the same data sheet as the sample placement information. The blank samples were
similarly processed.
5.4 Environmental Conditions
A rain gauge and a minimum/maximum thermometer were placed at fUC's site to monitor rainfall and
air temperatures during sampling in order to ensure compliance with the regulatory measurement
criteria.
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In accordance with 40 CFR, Part 61, Appendix B, Method 115:
. Measurements were not initiated within 24 hours of a rainfall.
. The seals around the lip of the collectors were not broken nor slurounded by water.
o The measurements presented in this report were not performed during temperatures below
35oF or on frozen ground (the minimum air temperature recorded at the site during the
collection periods was 50'F).
6. SAMPLE ANALYSK
6.1 Apparatus
Apparatus used for the analysis:
. Single- or multi-channel pulse height analysis system, Ludlum Modei 2200 with a
Teledyne 3" x 3" sodium iodide, thallium-activated (Na(Tl)) detector"
. Lead shielded counting well approximately 40 cm deep with 5-cm thick lead walls and a7-
cm thick base and 5 cm thick toP'
. National lnstitute of Standards and Technology (NIST) traceable aqueous solution radium-
226 absorbed onto 180 grams of activated charcoal.
. Ohaus Model C501 balance with O.l-gram sensitivity.
6.2 Sample Inspection and Documentation
Once in the laboratory, the integrity of each charcoal container was verified by visual inspection of the
plastic container. Laboratory staff documented damaged or unsealed containers and verified that the
data sheet was complete.
A total of four samples were lost in the field due to charcoal spillage. All of the remaining 396 sample
containers received and inspected at the Tellco analytical laboratory were verified as valid.
6.3 Background and Sample Counting
The gamma ray counting system was checked daily, including background and radium-226 source
measurements prior to and after each counting session. Based on calibration statistics, using sources
with known radium-226 content, background and source control limits were established for each
Ludlum/Teledyne cotrnting system with shielded well (Appendix A).
Gamma ray counting of exposed charcoal samples included the following steps:
e The length of count time was selected by the activity of the sample being analyzed,
according to a data quality objective of a minimum of 1,000 accrued counts for any given
sample.
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o The sample container was centered on the NaI detector and the shielded well door was
closed.
The sample was counted over a determined period and then the mid-sample count time
date and counts were documented on the field data sheet and used in the calculations.
The above steps were repeated for each exposed charcoal sample.
Approximately 10 percent of the containers counted were selected for recounting. These
containers were recounted within a few days following the original count.
7. QUALITY CONTROL (QC) AND DATA VALIDATION
Charcoal flux measurement QC samples included the following intra-laboratory analytical frequency
objectives:
r Recounts, 10 percent, and
o Blanks, 5 percent
All sample data were subjected to validation protocols that included assessments of sensitivity,
precision, accuracy, and completeness. All method-required data quality objectives (EPA, 2001) were
attained.
7.1 Sensitivity
A total of twenty blanks were analyzed by measuring the radon progeny activity in samples subjected
to all aspects of the measurement process, excepting exposure to the source region. These blank
sample measurements comprised approximately 5 percent of the field measurements. The results of
the blank sample analyses *.**rOiudon fluxiates ranged from less than 0.01 to 0.12 pCi/m2-s, with
an average of approximately 0.06 pCi/m'-s'
7,2 Precision
Forty recount measurements, distributed throughout the sample sets, were performed by replicating
analyses of individual field samples (see Appendix B). These recount measurements comprised
appioximately 10 percent of the total number of samples analyzed. The precision of all recount
measurements, expressed as relative percent diflerence EPD), ranged from less than 1 percent to 33.3
percent with an overall ayetageprecision of approximately 5.1 percent.
7.3 Accuracy
Accuracy of field measurements was assessed daily by counting two laboratory control samples with
known Ra-226 content. Accuracy of these lab control sample measurements, expressed as percent
error, ranged from -5.3 percent to 4.8 percent. The arithmetic average error of the lab conhol sample
measurements was -0.5 percent (see Appendix A).
7.4 Completeness
Ninety-eight of the samples from the Cell 2 Beaches Region were verified, representing 98 percent
compieteness for that region. All 100 of the samples from the Cell 2 Covered Region were verified,
representing 100 percent completeness for that region'
Ninety-nine samples from the Cell 3 Beaches region were verified, representing 99 percent
compieteness for that region. Ninety-nine samples from the Cell 3 Covered Region were verified,
representing 99 percent completeness for that region.
Altogether, 396 of the total 400 sample locations were verified during this sampling program,
representing 99 percent completeness overall'
8. CALCULATIONS
Radon flux rates were calculated for charcoal collection samples using calibration factors derived
from cross-calibration to sources with known total activity with identical geometry as the charcoal
containers. A yield efliciency factor was used to calculate the total activity of the sample charcoal
containers. lndividual fleld sample result values presented were not reduced by the results of the field
blank analyses.
In practice, radon flux rates were calculated by a database computer program. The algorithms utilized
by the data base program were as follows:
Equation 8.1:
pCi Rn-222hisec :
11r-a-t#5(d/er.75)l
where: N
Ts
b
: net sample count rate, cpm under 220-662 keV peak: sample duration, seconds: instrument calibration factor, cpm per pCi; values used:
0.1758, for M-01/D-21 and
0.1164, for M-021D-20: decay time. elapsed hours between sample mid-time and cormt mid-time: area of the collector. rnl
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Equation 8.2:
Erxor,2o = 2x
Gross Sample, cpm Background Sample,cpm
SampleCount,t,min Background Count,t,min x Sample Concentratfon
Net, cpm
Equation 83:
r-'o:ffiffi,*,,1
where:2.71
4.65
S6
Ts
b
= constant: confidence interval factor
= standard deviation ofthe background count rate
= sample duratiorl, seconds
= instrument calibration factor, cpm per pCi; values used:
0.1758, for M-01/D-21 and
0.1764, for M-02/D-20: decay time, elapsed hours between sample mid-time and count mid-time
: area of the collector, m'
9.
9.1
RESULTS
Mean Radon Flux
Referencing 40 CFR, Part 61, Subpart W, Appendix B, Method 115 - Monitoring for Radon-222
Emissions, Subsection 2.1.7 - Calculations, "the mean radon flux for each region of the pile and for
the total pile shall be calculated and reported as follows:
(a) The individual radon flux calculations shall be made as provided in Appendix A EPA
86(1). The mean radon flux for each region of the pile shall be calculated by summing all
individual flux measurements for the region and dividing by the total number of flux
measurements for the region.
(b) The mean radon flux for the total uranium mill tailings pile shall be calculated as follows;
JA+...JzAzt+l...JA
J.:
&
Where: J. : Mean flux for the total pile (pCi/m2-s) -
J; : Mean flux measured in region i @Cilmr-s)
Ai : Area of region i (m2)
At : Total area of the Pile (m2)
2.1.8 Reporting. The results of individual flux measurements, the approximate
locations on the pile, and the mean radon flux for each region and the mean radon flux for the total stack
[pile] shall be included in the emission test report. Any condition or unusual event that occurred during
th" rn"u.*.rrents that could sigrrificantly affect the results should be reported'"
9.2 Site Results
Site Specific Sample Results (reference Figure 2 and Appendix C)
(a) The mean radon flux for each region within the site as follows:
Cell2 - Cover Area
- Beach Area
Cell3-CoverArea
- Beach Areas
- Standing Liquid
6.6 pCi/mz-s (based on267,604 m2 area)
55,8 pCi/m2-s (based on 3,020 m2 area)
7.1 pCi/m2-s (based on 156,452m2 area)
74.2pCr/mz-s (based on 28,388 m2 area)
0 pCi/m2-s (based on 104,018 m2 area)
Note: Reference Appendix C of this report for entire summary for individual measurement results.
(b) Using the data presented above, the calculated mean radon flux for each cell (pile) is, as follows:
Cell2: 7.1 pCi/m'-s
(6.6X267.604) + (55.8X3.020)
270,624
Cell3: 6.2PCt/rrf -s
(7. 1)(1 s6.4s2) + (24.2)(28.3 88) + (0x 1 04.0 t 8)
288,858
As shown above, the arithmetic mean radon flux for the each cell at [UC's White Mesa milling
facility is below the NRC and EPA standard of 20 pCilm2-s. No condition or unusual event
occurred during the measurements that could significantly affect the reported results. Appendix C is
a sunmary of individual measurement results, including blank sample analysis. Sampfe locations are
depicted on Figure 2, which is included in Appendix D. The map was produced by Tellco.
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I References
I U. S. Environmental Protection Agency, Radon Flux Measurements on Gardinier and Royster
Phosphogypsum Piles Near Tampa and Mulberry, Florida, EPA 52015-85-029, NTIS #PB86-
I , :':I,?J,}:Tr'i,t"u,..,,", Agency, ritte 40, code of Federat Regutations,zolt.
U. S. Nuclear Regulatory Commissioq Radlological Effluent and Environmental Monitoring at
I (Jranium Mills,Regtlatory Guide 4.14, April 1980'
I U. S. Nuclear Regulatory Commission, Title 10, Code of Federal Regulations, Part 40, Appendix A,
I
July 1ee7.
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l0-in. dia
PVC End CaP
Figure 1
Large Area Activated Charcoal Canister Diagram
fIGURE I Large-Area Radon Collector
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Appendix A
Charcoal Canister Analyses Support Documents
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calibrationDate: Q / o r I o; DueDate: b I ot I OA
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System ID:
Scaler S,N:
Gross Source Range, cpm:
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The acceptable ranges were determined from prior background and source check data.
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{t srrn rocAn M$|,- M f se\ [q', t( - g | ^n d ,, j, L,t-f
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Appendix B
Recount Data Analyses
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