DRC-2006-001142 - 0901a0688080569a

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PARTICULATE MATTER COMPLIANCE TEST
CONDUCTED AT
INTERNATIONAL URANIUM (USA) CORPORATION
NORTH YELLOW CAKE SCRUBBER
BLANDING, UTA[I
June 27,2A06
t'Y:
TETCO
90 East Main
Lehi, UT 84043
Phone [phone]
Fax [phone]
Prepared for:
International Uranium (USA) Corporation
6425 S Hrvy 9l
Blanding, Utah 84511
Date of Report:
July 6,2006
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CERTIFICATION OF REPORT INTEGzuTY
Technical Emissions Testing Company (TETCO) certifies that this report represents the truth
as well as can be derived by the methods employed. Every effort was made to obtain accurate and
representative data and to comply with procedures set forth in the Federal Register.
Mike Ransom
p.a15-. '7- -/ --0 b
Dean A. KitchenReviewe,: k 4fr*
Date:7-6-e6
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TABLE OF CONTENITS
PAGE
IntroductionTestPurpose.... ....,... I
TestlocationandTlpeofProcess. .....1
TestDates ........1
PollutantsTestedandMethodsApplied ........1
TestParticipants. ........1
Deviations FrornEPAMethods .........2
QualityAssurance .......2
Summary of Results
EmissionResults ........3
ProcessData. .....3
AllowableEmissions .....3
Description of Collected Samples . . . . . . .4
Discussion of Errors orlrregularities . . .........4
Percentlsokinetics .......4
Source Operation
ProcessControlDevicesOperation ......5
ProcessRepresentativeness ......5
Sampling and Analysis Procedures
SamplingPortlocation.... .....6
SamplingPointlocation.. ......6
SamplingTrainDescription ......7
SamplingandAnalyticalProcedures ... ........7
QualityAssurance .....; ......-7
Appendices
A: Complete Results and Sample Calculations
B: Raw'Field Data
C: Laboratory Data and Chain of Custody
D: Raw Production Data
E: Calibration Procedures and Results
F: Related Correspondence
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LIST OF'TABLES
PAGE
TableI MeasuredPMEmissions ........3II Percentlsokinetics .......4III SamplingPointlocation.. ......6ry CompleteResults .....AppendixA
LIST OF FIGURES
Figure1 Facility Schematic Representation . . . . Appendix D2 Schematic of Method 51202 Sampling Train . . Appendix E
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INTRODIJCTION
Test Purpose
This test was conducted to determine the total particulate matter (PM) emissions from the
North Yellorv Cake Scrubber exhaust in terms of pounds per hour (lb/hr).
-, Test Location and Type of Process
I International Uranium (USA) Corporation is located about 5 miles south of Blanding, Utah.
Uranium ore is processed into yellow cake, which is shipped to other facilities for additional
I processing. There tue two yellow cake dryers with individual scrubbers. The North Yellow CakeI dryer was the only operating dryer at the time of the test. The South Yellow Cake Dryer is currently
not operational.
I A facility schematic is shown as Figure 1 in Appendix D.
I rest Dates
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All testing was completed June 27 ,2006.
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Pollutants Tested and Methods Applied
The tests were a gravimetric determination of particulate matter (PM) in accordance with
I EPA Method 5. Method202was run is conjunction with the Method 5 tests. Method 202isnot for
I compliance but for information only.
I Test Participants
I rest Fac,itv y#il ?;fr
State Agency Joe Randolph
TETCO Dean Kitchen
Mike Ransom
Joseph Kitchen
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Discussion of Irreglrlarities
The dryer shut down during run #2 without the knowledge of the test crew; therefore, the
process was not fully operation during this test run. A fourth test run was completed in orderto have
three acceptable test runs. Data for run #2 is included in the appendix for informational purposes
only.
Oualiff Assurance
Testing procedures and sample recovery techniques were according to those outlined in the
Federal Register and the Quality Assurance Handbookfor Air Pollution Measurement Systems.
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SIJMMARY OF RESULTS
Emission Results
Table I presents the findings of the compliance test in pounds per hour of PM. Table IV in
Appendix A has more detailed information.
Process Data
The process was operated according to standard procedures. All pertinent process data was
available for recording by agency personnel. Production data will be submitted by International
Uranium.
Allowable Emissions
The allowable PM emissions for this scrubber are 0.4 pounds per hour.
Descrintion of Collected Samples
All three test filters were lightly covered with a yellowish colored particulate. The front
washes were clear in appearance.
Percent Isokinetic Sampling
Each of the tests were isokinetic within the +10% of 100oh criterion specified in the Federal
Register. They also meet the Utah State Department of Environmental Quality, Division of Air
Quality specification of isokinetic sampling point by point. Isokinetic values for each test run are
presented in Table II.
Discussion of Errors
None.
North Yellow Cake
Scrubber
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souRCE OPERATTON
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Process Control Devices Operation
All process control devices were operated normally.
I Process Representativeness
I U.unir,]|.
facility was operated normally. Production data will be submitted by Intemational
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SAMPLING AND ANALYSIS PROCEDURES
Sampling Port Location
The inside diameter of the North Yellow Cake stack is 18.0 inches. The two, four-inch
diameter sample porl are located 6.3 diameters (9.5 feet) downstream from the last disturbance and
6.3 diameters (9.5 feet) upstream from the next disturbance. Figure I in Appendix D is a schematic
of the stack.
Samplins Point Location
Table III shows the distance of each sampling point from the inside wall according to EPA
Method l. Each point is marked and identified with a wrapping of glass tape and numbered. These
points are determined by measuring the distance from the inside wall.
Distance (inches) from Inside Wall
0.58
1.89
3.49
5.81
12.19
14.51
16.1 I
Sampling Train Description
To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-5
and 40 CFR 51, Appendix M, Method 202were followed.
All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent
interference of the sampled gas and particulate.
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The stack analyzers used to conduct Methods 1-5 and 202 arc constructed to meet the
specif,rcations outlined in the CFR. fhe temperature sensors are K-type thermocouples. Heater,
vacuurll and pitot line connections have been designed to be interchangeable with all units used by
the tester. A 316 stainless steel probe liner was used for the tests. Figure 2 in Appendix E is a
sketch of the Method 51202 sampling train.
Sample boxes were prepared for testing by following the prescribed procedures outlined in
Methods 5 and202.
Sampling and Analytical Procedures
All sampling and analltical test procedures were as specified in 40 CFR 60, Appendix A,
Method 5 and 40 CFR 51, Appendix M, Method 202.
Ouality Assurance
All equipment set-up, sampling procedures, sample recovery and equipment calibrations were
carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbook
for Air Pollution Measurement Systems.
APPENDIX
A: Complete Results and Sample Calculations
B: Raw Field Data
C: Laboratory Data and Chain of Custody
D: Rarv Production Data
E: Calibration Procedures and Results
F: Related Correspondence
APPENDIX A
Complete Results
Nomenclature
Sample Equations
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NoathYollowake
TABLE iV
COMPLETE RESULTS, PM
TNTERNATIONAI- URANTUM CORPORATION (tUC)
NORTH YELLOWCAKE SCRIJI]BER EXHAUST
Syrnbol
Date
Filter #
Begin
End
Pbn,
AH
Y
Vtn
'fn'
iap
wr*"
Tr
ce
D"
CO,
o2
N2&CO
Vm.,6
Bw,
x,r
M,r
M.
%t
T"
A,
PC
Pb,
P.
a,
Q"
Mnt,",
Mp
MF
MB
cr
Cb""t
ERt
Erto"r
Dimensions Run #l Run #3
612'7106 6t27 t06
4760 4762
7:17 12:02
8:56 12:58
21.63 24.63
r.339 1.109
1.002 r.002
46.531 44.106
77.7 103.5
0.2839 0.2746
12r.8 134.8
64 64
0.84 0.84
0.3700 0.3700
2.20 2.80
t7 .40 r 7.00
80.40 80.20
37.839 34.20t
s;743 6.356
0.1258 0.1s26
0.874 0.847
29.05 29.13
27.66 27.43
106.7 103.1
|6.2 123.1
,.767 1.76'l
-0.03 -0.03
24.6i 24.63
24.628 24.628
l.3lE+03 t.23E+03
1.99E+03 I .94E+03
l.l3E+03 l.t0E+03
Run #4
6t27 t06
4786
l4:15
l5:20
24.63
t.076
1.002
42.808
104.3
0.2708
135.2
64
0.84
0.3700
2.60
t7.40
80.00
33. l 48
6.37s
0. r 606
0.839
29.11
I t:3
102.3 AVG
125.0 121.4
1.',l67
-0.03
24.63
24.628
1.208+03 1.258+03
1.92E+03 t.958+03
t.09E+03 l.l0E+01
t6.6
8.8
25.4
I.5
0.01r8 0.01r6
0.0007 0.000s
0.t2 0.12
0.0072 0.0047
F Run #2
o 6/27t06
R 476r
9:56
1 l:02
I 2s35
N 1 .168
F 1.002
o 43.056
R 93.6
M 0.2676
A 99.5
T64
I 0.84
o 0.3700
N I-60
18.60
79.80
34.980
4.691
0. Il8
o 0.882
N 29.00
L 27.70
Y 102.8
I 16.8
26.725
-0.29
2s.20
25.179
1.908+04
2.808+04
1.058+03
8.7
I8.l
26.8
0.5
0.0r l8
0.0002
1.93
0.0360
Description
Date
Trme Test Began
Time Test Ended
Meter Barometric Paessure
Orifice Pressure Drop
N,leter Calibration Y Fa.tor
Volume Gas Sampled-Meter Conditioos
A\'g Meler Temperature
Sq Root Velocity Head
We;ght Water Collected
Duration ofTest
Pitot Tube Coeflicienr
Nozle Diameter
Volume % Carbon Dioxide
Volume o/o Orygen
Volume oZ Nitrogen and Carbon Monoxide
Volume G6 Sampled (Standard)
Volume Water Vapor
Fraction H20 in Stack Cas
Fraction ofDry Cas
IVolecular Wt. Dry Cas
Molecular WI Stack Gas
Percent lsokinelic
Avg Slack Temperature
Stack Cross Sectional Area
Slack Static Pressure
Sample Pod Barometric Pressure
Stack Pressure
Stack Cas Volumelric Flow Rate (Std)
Stack Gas Volumetric FIow Rate (Actual)
Velocity ofStack Cas
Mass ofPadiculate on Filter
lvlass of Paniculate in Wah
lv{ass of Front Half
h4as olBack Half
Concentration of Front Half
Concentration olBack Half
Emission Rate offronl Half
Emrssion Rate ofBack Half
ln tlg Abs
ln lllo
dimensionless
cf
.,F
Root ln. HrO
Grms
lviinutes
Dirnensionless
lnches
Percent
Percent
Percenl
dscf
scf
Fraction
Fraction
lb/lbmol
Ib/lbmol
Percent
.,F
Sq. Ft.
In H;O
In Hg Abs
In Hg Abs
dscfm
cfm
fp.
milligrams
milligrms
milligrams
milligrams
gr / dscf
gr / dscf
lb/hr
Ibihr
9.2
20.7
29.9
0.5
15.7
8.5
74.2
1.0
0.0122 0.0109
0.0002 0.0005
0.14 0.1 I
0.0023 0.0047
Salurated moishrre liaction used in all calculations for runs l, 3, & 4 as the measured moishrre was supersatumted
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M5 &202 Nomenclature
o/ol : percent isokinetic, percent
A, = stack cross-sectional area (ftl)
ASAP: s"" lAP
BtLr : unit heat value (British thermal unit)
B,u, : fraction of water in stack gas
Cs = concentration of parliculate matter. back half (grldscf,lb/dscf, etc.)
C.on,l : concentration of condensibles (grain/dscf)
C; = concentration of particulate matter, front half (grldscf,lb/dscl etc.)
C*.t.t : concentration of metals (ppm, pg/ft3, etc.) atomic symbol replaces "metal,,
CO: : percent carbon dioxide in the stack gas
Co : pitot tube coefficient (0.84)
C.y lnugy = species syrnbol replaces x.
C.r.(.on) : actual gas concentration corrected to required percent 02
AH : orifice pressure drop (inches H2O)
AHO = orifice pressure (inches H2O)
D,: nozzle diameter (inches)
AP : stack flow pressure differential (inches H2O)
D, : diameter of the stack (feet)
EA : percent excess air
ERs: emission rate of back half particulate (lb/hr)
ER.o^ : emission rate of coarse particulate (lblhr)
ERp : emission rate of front half particulate (lb/hr)
ERr*g,, : emission rate per mmBtu or ton of fuel etc.
ER.r. : emission rate of compound which replaces x
k-fact = multiplier of test point AP to determine test point AH
L : length ofrectangular stack (inches)
mBtu : thousand Btu
M.ond : mass of condensibles (milligrams)
M6 : rnolecular weight of stack gas, dry basis (lb/lb-mol)
Mo = mass of particulate on filter (mg)
Mpp: mass of parliculate matter on filter and probe (mg)
rnmBtu: million Btu
Mo : mass of particulate matter in probe (mg)
M, : molecular weight of stack gas, wet basis (g/gmol)
N2 : percent nitrogerr in the stack gas
02 - percent oxygen in the stack gas
{AP : average of the square roots of AP (may also be referred to as ASAp)
Pb,, : absolute barometric pressure at the dry gas meter (inches Hg)
Pbo : absolute barometric pressure at tlre sample location (inches Hg)
P6 - stack static pressure (inches H2O)
P, : absolute stack pressure (inches Hg)
P*,,1 - absolute pressure at standard conditions {29.92 inches Hg.)
0: time of test (minutes)
Qo : stack gas volurnetric flow rate (acfm)
Q, : stack gas volumetric flow rate (dscfm)
Qw : wet stack gas std. volumetric flow 1ft3/min, wscfm)
t M5 &.202 Nomenclature
I *: ;f,:i:#il:TJ:)u,uunau.a conditions (s28"R)
I X: ;lu? morecurar speed (cmis)
Vm : sample volume 1ft3; at meter conditions
I "'t: ;:H;:?if::ffi;, prevorumeadjustedto6s'F and2ee2inchesHg
I "il: ;ilililH,-ffi*-" li,i;nd2e
e2 inches Hg
Wt,u.: rveight of the condensed water collected (grams)
I t= Iliji"J,;illff'".ctor(dimensionress)
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I Method 5 &202
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o%t: Vm,,6. (T,+460).1039/(e.v,.p,.Xo. pnz;
A, = (Ds2 I 4). r
I .'-: = I-:i:il;i l,u;/,**,
C.or. : M.,,r, . 0.01 543 / Vmr,4
I ., ,."11: Ijl-j :ii;i i Il;::, %o2) , e0 s - actvat.ho.)
D..,:2'L'Wi(L+W)l,;x: [!].,i,;ff;ii{;i}"!{,:ii,iil;:iJs;,,r(r,+460)-M,)/(p..^p),}I 'til = !::'"3;,Xli;"
ER,.tsr, : ER* / (nrmBtu / hr)
I K-fact: 846.72. Dn4. aH^. gr2. xo'. Ma. p,. (T* + 460) / [Ms. (T, + 460). (pb, + AH / 13.6)]f M,i - C0. '0.44 +or'0.32 + N: .0.28
I Y:: iY, ;;:,.,::; '-''
Q.: V,'A,
I tT: 3:;#
' Ps'r"4 / r(rs + 460)'P..'tl
Vfl,ta = Vm. Y. T,rd. (Pb. +AH/ 13.6)l [Poo. (T. +460)]
I ;': i,i,il.'r:ffii''rap'! 11r' + 460) / (P" M')l
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X6= r-B,u.
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T APPENDIX B
I i;llffi:?y"yJlB':1J*"rse
and sampring Point Location Data
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Averages:
Z Flow
.lap
TS
AP
zFbo-'4 D
AP
N
Stack Dia. l8
Ports are 9.5'
Ports are 9.5'
Rel'erence 0.0
Upstream lrom next disturbance
Do$nstream tiom Iast disturbmce
Prelim North Yellowcake
Comments:
Facility International Uranium
Stack Identification North Yellow Cake Drver Scrubber
Date ,- -Z C ' d L
Barometric Pressure
Pb*-- in Hg Pb, in Hg
Static Pressure po1 - . a3 in UrO
Estimated Moisture (Bw,) 4-6 o/o
Sample Height from Ground 50' feet
Time:
Traverse
Point
Percent
Diameter
Distance From:Ports
TD Reference A B C D E F'
3.2 0.58 0-58 ?)-oC , ?l-
2 t 0.s 1.89 1.89 ,eJ-A
)19.4 3.49 3.49 f 1fa?1 ,?{ 7
4 32.3 5.81 5.81 ,e7 9f ,q
5 67.7 12.19 12.19 ),r, ?1 ,// v
6 80.6 14.5 1 14.5 t ',t/ E ./3 ry
7 89.5 I6.l I 16.11 I ,x etl ./t/ u
8 96.8 17.42 l7.42 ft,,/ 'r
KEY ->
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APPENDIX C
Sample Recovery
Particulate Analysis Sheets
Condensible Particulate Analysis Sheets
Gas Analysis Data (ORSAT)
Chain of Custody
Facility: International Uranium
Stack Identification: North Yellow Cake Scrubber
Filter Number:4760
Date:6/27106
Run:
Sample Box:
BIanksBlanks &
Rinses Acetone (cHrcocH3) 0.0001 g/100m1 Acetone (CHrCOClir) 225
Filter Final,:
Final,:
0.6806
0.6807 ob
Date: 7/3106
Date: '7/5106
Time: 10:00
Time: 10:00
Final.al'6:
Filter newetghr:
Net
Net
0.6807 C
0.6715 g
0.0092 s
mg
CzuTERIA
Process Weight Time
Fina Pass Pass
lr
I
t.1
Il
It
tt
ll
lt
TI
il
ll
ll
l;
I
l-
l-
t-
t
Front Half
Final,:
Finalr:
Initial,:
Initial2:
Beaker Nun'rber:
125.3804
t25.3804
ob
ob
ob
Finalay6: 125.3804 g
125.3593
Date
Date
Date
Date
Time: 10:00
Time: 8:00
Time: 10:00
Tin're: 9:00125 3596 6/7t06
33
Initial4y6:
Gross.
Blank:
125.3595 g
0.0209 g
0.0002 C
Net_ 0.0292_8
Net 20.7 mg
CITITERIA
Process Iime
Fina
Initia
Pass
Pass
Pass
Pass
RESULTS Front Half
Filter 9.2 mg
Wash 20.7 mg
Total 29.9 mg
COlfftnents: Critc-ria: l)Weightsue+05mgofeachother,orwithinlo/oofthenetweight 2)Thereshallbeatleast6ltrsbctweenweiglungs
Lab Technicia ", U4 Date:7-5'oz5
Dare:7 - 7'e6I
t
Lab Technician, fu/R
I
I sto"rra",t,lllll3,*ffi
Filter Number' 4761
Date: 6/27106
Run: 2
Sample Box: E
Blanks & Blanks
Acetone (CH3COCHT) 0.0001 g/100m1 Acetone (CH,CoCH3) 195 nrlRinses
Filter Finall: 0.6699 g
Final2: 0.6699 g
Finaloy6: 0.6699 g
Filter *"r"ight: 0.6612 C
Nct 0.0087 g
Net 8.7 mg
Date: 1/3106 Time: 10:00
Dare'. 715106 Time: 10:00
CRITERIA
Process Weighl Time
Fina Pass Pass
t
ll
tt
tt
Front Half
Finall: I 01. I 375 g
Final.: 103.1376 C
Initiall: 103.1l9l g
Initial2: 103.1l9-5 C
Finalay6: 103.1376 g
Date: 715106 Time: 10:00
Date: 7/6106 Tirne: 8:00
Date: 616/06 Time: 10:00
Dare: 6/7106 Time: 9:00
CRITERIA
Process Weight Time
Fina
lnitia
Pass
Pass
Pass
Pass
Initialor6: 103.1193 g
f 1 G'oss,--oITE5-g
I I neaker Nurnber: 34 Blank: 0.0002 g
Net 0.0181 g
Net 18.1 mgll
tl
ll
t_
l_
l-
t'
t;
BESULTS
Filter 8.7 mg
Wash l8.l mg
Total 26,8 mg
COtnrfrentS: Criteria: l)weights_I9_*_91 -gq"""hlth9l-*,ft-1%ofg:nelreighl 2Ag"thrttb"",t"^,6k
tr
Lab rechnicia ,, 0 /l Darc: 7 -6 -o C
Labreclrnicia n, %K Darc:7 - 7 ' ob
I
I Facility: International Uranium
Stack Identification: North Yellow Cake Scrubber
Filter Number: 4762
Date: 6/27106
Run: 3
Sarnple Box: F
I Bt"rk, &
Rinses
BIanks Rinses
Acetone (cH3cocHr) 0.0001 g/100m1 Acetone(cHrcocHr) 215 ml
I Filt.r i"*rtr,--- o.oux ,I nirut,,----TZEa-g
Date: 713106 Time: 10:00
Date: 715106 Time: 10:00
CRITERIA
Process Weighl Trme
Fina Pass Pass
Finaloy6: 0.6'796 g
Filter n"'ue;gtt: 0.6639 C
Net 0.0157 g
Net 15.7 mg
t
I
t
I
Front Half
Finall: I 16.9784 g
Final.. 116.9782 C
Finalay6: 116.9783 g
InitialAvc: 116.9696 g
I Gross: 0'0087 g
I Beaker Number: 35 Blank: 0'0002 g
Date: 715106 Time: 10:00
Date: 716106 Time: 8:00
Date: 616106 Time. 10:00
Date: 617106 Time: 9:00
CRITERIA
Process Weisht Time
Fina
Initia
Pass
Pass
Pass
Pass
Initiall. 116.9698 g
Initial.: I 16.9694 C
Net 0.0085 C
Net 8.5 mgT
I
l'
I
T
t;
li
BESULTS Front Half
Filter 15.7 mg
Wash 8.5 mg
Total 24.2 mg
CCI-rrerts q!-, tjt *,*"..t',-r ' *'
Lab Teclrnicia n: / /(oate:7-6'3C
LabTeclrnicia n ? K oarc, 7- 7'o4
I
I
I
Facility: International Uranium
Stack ldentification: North Yellow Cake Scrubber
Filter Nunrber:4786
Date:6/27/06
Run
Sample Box: D
RinsesBlanksBlanks &
Rinses Acetone (CHlCocHr) 0.0001 g/l0Oml Acetone (CHiCoCHr)200 ntl
t
I
I
Filter Finall:
Final2:
0.6244
0.6248
g
o
Finalay6. 0.6246 g
Filter rre'veight: 0.6080 C
Date: 713106 Tirne: 10.00
Date: 715106 Time: 10:00
CRITERIA
Process Weisht Time
Fina Pass Pass
Net 0.0166 g
Net 16.6 mg
Front llalf
6t6lo6
Net
Net
35
I
I
I
I
rt7.2761 Date:
Date:
Date:
Date:
'7 t5t06Finall:
Final2:
Initiall:
Initial2:
1t'1.2763 7/6t06
Time: 10:00
Tirne: 8:00
Time: 10:00
Time: 9:00
tt"t.26'70
Finalay6: 117.2762 g
111.2612 g
617106t17.26'73
lnitialay6:
Gross:
Blank:
9e0.0002 g
0.0088 s
8.8 mg
CRITERIA
Process Weight Tme
Fina
Initia
Pass
Pass
Pass
Pass
RESULIS Front Half
Filter 16.6 mg
Wash 8.8 mg
Total 25.4 mg
I
I
I
t
I
t
I
Corntuents L-riteria: l ) Weights are + 0.5 mB of each other, or within l ozi' of the net weight 2) There shall be at le6t 6 lrs betwftn
Darc: 7 - tr*ac
Date: 7 - 7-O4I;
td
Lab Technicia " /4
International Uranium Date:
rl 202
6t27 t06Facility
Stack Identification
Filter Numbet
North Yellow Cake Scrubber
4760
Run:
Sample Box:
BIanl<s RinsesBlanks &
Rinses Water iH,o) 0.0000 g/100nl1
Methylene Chloride (CHrcl?) 0.0001 g/100m1
Watere 1urol 800.0 g
Waterl 1nrol 529.0 g
Water (Ilro) Net* 571.0 ml
Methylene ChlorideF (CHrctrl 365.0 g
Methylene Chloride, lcHrctrl 174.0 g
Meth,vlene Chloride (CH,CI2) Net* 294.7 ml
*lncludes volumes for Impinger set-up (300m1 H2O) and analysis (150m1 CH2CI2)
I
I
!
I
I
I
I
I
T
t'
I'
t
t.
I
I
Water
Analysis
165.8676Finali:
Final2:
Initiall:
Initialr:
Beaker Number:
165.8675
ob
gb
Finalay6: 165.86'76 g
1t5/06
'il6t06
Date: 5123/06 Tirne: 17:00
Dare: 5126/06 Tirne: 9:00
Date:
Date:
Time: 10:00
Time: 10:00
165 8673 ob
ab165.8674
405
Initialay6:
Gross:
Blank:
Net
Mi Net
165.8674 g
0.0002 C
0.0000 C
0.0002 C
0.2 mg
CRITERIA
Process Weighl Time
Fina
Initia
Pass
Pass
Pass
Pass
Titration 6.50pH
Csoa
\4
Mi
Normalitv
Titrant
Vi"
N NH4OH
mV,
rnl
Vi. .- Init'al vol H2O in impingen + total grams caught in impingem
M,-M"
- net silica gel wt + net rinse volume
= 48.03 . N'V, / 100
= 0.0205 . Csoa . Vi"
Methylene
Chloride
Analysis
Finall:
Final2:
Initiall:
Initial2:
Beaker Number
I 75.5559
175.5555
ob
175.5550
175.555 I
Gb
c
Finalal,6: 175.5551 g
Date: 715106 Time: 10:00
Date: 716106 Time: l0:00
Time: l7:00
Tirrr".---6ffi-Date: 5126lA6
Date: 5123106
406
Initialoyo:
Gross:
Blank:
Net
175.5551 C
0.0006 C
0.0003 C
__0.0m1_e
0.3 mg
CRITERIA
Process Wei8ht T"me
Fina
Initia
Pass
Pass
Pass
Pass
RESUTTS Mi 4.2 mg
ttlo--OJ-*g
Total CPM 0.5 mg
COmruentS: qgl]]I9,shl"r9l 0.1mg01 eachother,orwithinI?;ofthenetweisht 2)ft*lt"llg"ttry!:.!1."":*tg!Te.
Lab rechnicia ", ///Z-Darc' 7-6.o C
li
I
-24 t€Lab Teclmician: '- z ' \Dare'.V- 7- o 6
t2702
I FacilitY:
Stack Identification:
Filter Number:
International Uranium Date 6/27t06
North Yellow Cake Scrubber Run;
Sample Box:4761
Blanks &
Rinses Water (Hro) 0.0000 g/l00ml
Methylene Clrloride (cHrclr) 0.0001 g/l00ml
WaterF (II2O)
Waterr (H2O)
Water (ll2O) Net*
782.0 C
496.0
5860
MethyleneChlorideF(CHrclr) 368.0
Methylene Chloride,lcttrcl,l 172.0
Methylene Ctrloride (CHrClr) Net* 298.5
*lncludes volumes for Impinger set-up (300m1 H2O) and analysis (l50nrl CH2Clr)
ob
ml
o
ob
ml
Water
Analysis
Finall.
Final2:
Initiall:
Initial2:
131.7430 Date: '715106 Time: 10:00
t31.7 431
Date:
Date:
b
ob
dt)
oo
Finalay6: 131.7431 g
Date: 716106
5/23tO6
Time: 10:00
Time: 17:00
Time: 9:00
r31.7426
r3t.7 426
Beaker Nurnber: 407
Initialay6:
Gross:
Blank:
Net
Mi Net
131.1426 g
0.0005 c
0.0000 g
_ Loool_e
0.5 mg
CRITERIA
Process Weight Time
Fina
Inilia
Pass
Pass
Pass
Pass
Titration pH
Csoa
6r0
Normaliry
Titrant
Vt"
N NH4OH
mV,
ml
=4803.N'Vr/100
M"_= 0.0205 ' Csoa'Vi.
M,
-=M,-M"
Vi. : lnitial vol H2O in impingers + lotal gram cauglrt in impingem - net silica gel *t + net rime volume
Methylene
Chloride
Analysis
Finall:
Final2:
Initial,:
Initial,:
Beaker Numbcr:
t71.7606
1717607
gb
o
171 7602
171.1607
ob
o
Finalay6: 171.7607 g
Date. 115106 Time: 10:00
Time: 10:00Date: 716106
Date 5123106 Time: 17:00
Date: 5126106 Tirne: 9:00
CRITERIA
Process Weighl T'me
Fina
Initia
Pass
Pass
Pass
Pass
408
Initialay6:
Gross:
Blank:
Net
171.7605 g
0.0002 s
0.0003 C
0.0000 C
0.0 mgMo
BESULTS Mi
Mo
Total CPM 0.5
05 mg
mg
mg
00
Cournrenls
Lab Technicia r, ?K Dut".V-v-o6
t"
t
Critena: l)Weightsare+0.5mgofeachother,orwithinl%ofthenetweight.2)Thereshallbeatle6t6ksbelweenweiglung
Lab Tcchnicia ", /4 Date: 7-6 'o /^
l=
I
Facility:
Stack ldentification.
Filter Number:
International Uranium Date:6t27106
North Yellow Cake Scrubber Run:
Sample Box:4762
Blanks &
Rinses Water(HrO)
Methylene Chloride (cH?cl?)
t)
ob
ml
g
o
ml
0 0000
00001
g/l00ml
g/100ml
Watere 1llrOl 83-1.0
Waterl iHrot 532.0
Water lHro; Net* 602.0
MethyleneChlorideplcurctrl 362.0
MethyleneChloridellcnrctr; 174.0
Methylene Chloride (CH?C\ ) N.t* __22.4_
*Includes volumes lor Impinger set-up (300m1 H2O) and analysis ( l50ml CH2CI2)
Water
Analysis
Finall:
Fina12.
Initiall:
Initial2:
131.8371
r3l 8371
r3l 8359
r3l 8363
Beaker Nun.rber: 409
Finalay6:131.8371 g
Initialay6: 131.8361 g
Gross: 0.0010 g
Blank: 0.0000 g
Itet_,0.,00]9_g
Mi Net 1.0 mg
Date:
Date:
t
b
ob
ob
Date: 7 /5106
Date: 7 /6106
5t26tA6
Time . 10:00
Time: 10:00
Time; 17;00
Time. 9:00
CRITI]RIA
Process Weishl Tifie
Fina
Initia
Pass
Pass
Pass
Pass
I
I
I
t
I
I
I
I
I
T
T
I
I
I
I
l.
I
l;
I
Titration pH
Csoa
I\4
Mi
6.40
Normality
Titrant
Vi.
N NH4OH
mV
ml
=48.03.N.Vt/100
= 0.0205 . Cso4 . Vi"
= M, - IvI.
Vi. : Initial vol H2O in impingers + lotal grams caughl in impingers - net silica gel ut + ne1 rime volume
Methylene
Chloride
Analysis
Finall:
Fina12:
Initiall:
Initial2:
Beaker Number
t73.4225
r73.4222
b
b
Date:
Date:
Date.
Date:
'il5/06
716/06
Time: 10:00
Time: l0:00
Tirne: 17:00
Time: 9:00
Finalay6: 113.4224 g
173 4223
t'13 4224
ob
<tb
5123106
410
Initialay6:
Gross.
Blank:
Net
113.4222 g
-0.W g
0.0003 g
0.0000 S
mg0.0
CRITERIA
Proces weighl Tme
Fina
Inilia
Pass
Pass
Pass
Pass
BESUTTS Mi 1.0 mg
tuto---O.O-rng
Total CPM 1.0 mg
Comrnents
Lab Technicia". 4<Date.7-7- o{
ae + 0.5 mg ofeach other, or rvithin l% ofthe net weight 2) There shall be at least 6 ttrs between
LabTechnician, y'4 7,6-ao
I
I stacrraent,lllll"T,ffi
Filter Number. 4762
Date: 6/271A6
Run: 4
Sample Box: D
I Bt-rk, &
Rinses
I
I
Water (H,o) 0.0000 g/l00ml
Meth-vlene Chloride (cHrclr) 0.0001 g/l00ml
WaterF (H2o) 812O g
Water, {Hrol 5J-1.0 g
Water (H2O) Net* 355.0 ml
Methylene Chloridep lcH,ctr; 336.0 g
Methyiene Chloridel (CilrCtrl l7 5.0 g
Methylene Chloride lcttrclr) Net* 272.0 ml
tlncludes volumes for Impinger set-up (300m1 H2O) and analysis (l50ml CH2CI2)
gb
o
79
80
27
27
35
35II fJ;,I* :i::1,
Date 715106 Tirne: 10:00
Date: 716106 Time: 10:00
Date: 5/23106 Time: 17:00
Date: 5126106 Time: 9:00
CRITERIA
Process Weisht Time
Fina
Inilia
Pass
Pass
Pass
Pass
I Finalay6: 135.2180 g
I nitial, : 135 .27 65 g
Inirialr: 135.2769 c
Initialay6: 135.2767 g
c.orr, --610-T5-gI Beaker Number: 4ll nta*:-fiTdo-g
Net 0.0013 e
Mi Net 1.3 mgI
I
Titration
I
pH 6.00
N NH4OH Csoa = 48.03 - N' Vr / 100Nonnality
Titrant
Vi"
mV,
ml
N4_= 0.0205 . Csoa. Vi.
M,-= M, - M"
Vi. : Iritial vol H2O in impinges + lotal grams caught in impingem - net silica gel wt + net rinse volume
I '
LT,'31"J' Illlll,-j3#i, x
Finalay6: 112.0116 g
Date: 715106 Time: 10:00
Date: 716106 Tirne: 10:00
Date: 5/23106 Time: 17:00
Date: 5126/06 Time: 9:00
CRITERIA
Process weight Tirne
Flna
Initia
Pass
Pass
Pass
Pass
^ Analysis
I Initirll: 172.07 l0 g
Initiall: 172.0"71I g
r " I'"'3',;::,1ffi#-:
f Beaker Nutnber: 412 Blank: 0.0003 g
Net 0.0002 C
Mo Net 0.2 mg
" BESULTS Mi 1.3 rng
',t"rc#-**ili
I
Comments: Crireria: 1)lVeightsdenO5mgofeachother,orwithmlo,'oofthenelweight.2)Thereshalibeatleat6hrsbetweenweighings
I
T
Lab Technicia " /4 Dare: 7'f,- /6
Labrechnicia n.4K Date: 7- 7- o{
:,
.: Facility: .L U C.
ack ldentifica rron *- r.',t::;
II4PTNGI.RS
Run: J .Sample no*, D
rinat 365 g
Initial / 7 4
I n itials
i'
,?4 R
Total 1gy
HrO -:- - -. -_- -'_ -CHrCr;---- -- ':---'-*--:
r;nat T0O s
Initial 5Z ? g
Net Nel
E
I + l-32 -e'ml -
umber:
Initial Volume of liquid (HrO) in impingers, (ml)I
T
I
I
t
I
I
I
I
I'
t
a
I
t
I
t
l"
I
nun: 2..
Final 1gi
Initial 1g1
N:t (g)
Total 19;7 7, a-
Sanrple Oo*, €
I n iti als
+tK
Finat 7f)- e
tnttial?1f g
Finat ) {3r s
tnitial 17 Z e
_ -|.1,_ e Net
_ E+ t.32s/mt- mr
Run: )
I nitials
//,//--_a-
Final (gl
Initial (g)
Net 1s1
ro,utts*_J2 (,._{__
HrO
rinat 73 / ,
tnitiat 5)T s
Net e
cHrci, -
2aFinal ) LL r
tni,iotj7q - r
Net 1t - I.32 pr'ntl =:'l
Initial Volume of liquid (HrO) in impingers, (ml)
lnitial Volume of liquid (H,O) in i
L Uq , 'Date:
Method:'t/ZaZ
t, -) 7-zc-// t //o ),
I
I
I
I
I
I
I
IIUPINGEBS
Filter Number:
Tl Ztr[I n itials
/2._
4tt<Final 1gy
Initial 1_q1
Net (g)
RINSES H:O
rotat 1s1 / 1J;A
Firat ?!L I
lniriut -79I,
cH2cl2
ri,,ot 3 55 e
tnitial / 75 e
Net Net g + 1.32 g'ml =
lnitial Volume of liquid (H2O) in i.pir4.rsj*D
I
T
T
I
t
I
uuiuesfu:-
Filter Nunrber:
Run:Sanrple 13ox:
6
I
*8+1.32lnl'
.I nitials
Final 1g1
lnitial 1gy
N:t (g)
Total 1g1-BINSES , -*---'Hr6* ------ ---_-_=-cHrct
Final e
Initial g
Net
Final
lnitial
Net
Initial Volume of liquid (HrO) in impingers, (ml)
IMPINGEBS
Filter Number:
Sample Bo*i_
t
I
I
I
I
t
I nitials
iirNSeS
Final
Initial
Net
I
I
Final
Initial
Net
I
':'11':^l _
I
t
Initial Volume of liquid (HrO) in impin-qers, (ml)
I
t
I
il: r'/'j to"^ton /or// /,/L-,./, /a,"r//.-
Date 027-O6t "-l:Jil: ,+.
Ambient temp 79
t
I
T
I
I
I
I
T
Date 6)7-OG
Test No.-rl-
Cas BagNo. L"O'I
Ambient t"^r-|V-gp"rutu--ffi-
Operator /2//
Dare 6 )7 05
------------+-Cas Bag No. /z/-O)
Ambient Temp fd
Op"rutor--TW-
I
l"
I
t
t
l;
t
CO is not measured, as it has the same molecular weight as N2
Gas
RUN
Average
Net
Volume
2 J
Actual
Reading
Net Actual
Read i ng
Net Actual
Reading
Nel
CO,L.t^Az ).),z"z ),)^)-Z },L
O, (Net is Actual 02
Reading Minus Actual
CO2 Reading).
/7, e n//1.6 / /.r / 7,f,/ 7.7 /7.'/
N2 (Net is 100 Minus
Actual 02 Reading).
Gas
RAN
Average
Net
Volume
I 2 J
Actual
Reading
Net Actual
Rrnding
Net Actual
Reading
Net
CO,/,{/"r /"6 /.6 /e /,{/"r
O2 (Net is Actual 02
Reading Minus Actual
CO, Reading).
/o.L /tr6 7 0.2 /u6 2a.)/z{/t{
N, (Net is 100 Minus
Actual O, Reading).
Gas
RUN
Average
Net
Volume
I 2 3
Actual
Readins
Nct Actual
Reading
Net Actual
Re ading
Nct
CO,)"tr Af ),r )"/),r .L"tr 2,.0
02 (Net is Actual 02
Reading Minus Actual
CO, Readins).
,7, r t7, o /7.r /70 / /.//za /2a
N2 (Net is 100 Minus
Actual 02 Reading).
I
I
I
I
I
I
t
T
T
I
I
t
Plant
Anallical Method____=QRS4I__
Lo"ution /zz// /r//*- C,/, Jr.o//u-
Date f, lZ-/{
Test No. -1f-curaugwo.--V1V7-
Ambient l"^p-*/O '
operator ////i
Date
Test No.
Cas Bag No.
Ambient Temp
Operator
Date
Test No.
Gas Bag No.
Ambient Temp
. Operator
I
I
I
I
I
I
t
Gas
RUN
Average
Net
Volume
I 2 J
Actual
Reading
Net Actual
Reading
Net Actual
Reading
Net
CO,/.(2.I z-{2-{)"{2.{zd
O, (Net is Actual 02
Reading Minus Actual
CO, Reading).
) 2.o //./LA-O ///2d.o //.r /2?
N2 (Net is 100 Minus
Actual 02 Reading).
Gas
RUN
Average
Net
Volume
t 2 3
Actual
Reading
Nel Actual
Readins
Net Actual
Rcadine
Net
O, (Net is Actual O,
Reading Minus Actual
CO, Reading).
N, (Net is 100 Minus
Actual O2 Reading).
Gos
RUN
Average
Net
Volume
2 3
Actuel
Reading
Net Actual
Readins
Net Actuel
Re ading
Net
CO,
O, (Net is Actual O,
Reading Minus Actual
CO, Reading).
N2 (Net is 100 Minus
Actual 02 Reading).
CO is not measured, as it has the same molecular weight as N2
TETCO Stack Emission AnalYsis .(11
Acaiate o Reliable . Qualified tjl(j
90 East Main, Lehi, Utah 84043 o 801-768-0973 o FAX [phone]
Sample Identification
Chain of Custod
_-yg!99_9{4I4E!_ RecoveryDate
EPA Method 5 /Gravimetric t )7-A f
EPA Method 5
Samnle Descr iotion
Filter
Probe Acetone Wash
Impinger Catch and
HzO Rinse
CHzClz Rinse
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Probe Acetone Wash
Impinger Catch and
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Probe Acetone Wash
Impinger Catch and
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L{76/
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Filter
Gravimetric
EPA Method 202
Gravimetric
EPA Method 202
Gravimetric
EPA Method 5
Gravimetric
EPA Method 5
Gravimetric
EPA Method 202
Gravimetric- EPA Method 202
Gravimetric
EPA Method 5
Gravimetric-EPA Method 5
Gravimetric
EPA Method 202
Gravimctric-EPA Method 202
Gravimetric CHzClz Rinse
tr' 6 O Filter
6 ,z -acDate:
Date:
Date:
Date:
Date:
Date:
Date:
Sampled by:
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Relinquished by:
Received by:
Relinquished by:
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Analyzed By:
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90EastMain,Lehi,utah 84043 . 801-768-0973 0 FAX [phone]
Chain of Custody
,4/ /6
Sample Identification Method of Analysis
EPA Method 5
Gravimetric
Recovery Date
[.]7-of
____Samplglqgliption _
Filter
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Irnpinger Catch and
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CHzClz Rinse
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EPA Method 5
Gravimetric
EPA Method 202
Giavimetric
EPA Method 202
GravimetriccH2cl2
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Gravimetric Filter
Front EPA Method 5
Gravimetric Probe Acetone Wash
HrO EPA Method 202' Gravimetric
Impinger Catch and
HuO Rinse
CHzClz RinsecFl2cl2EPA Method 202
Gravimetric
Filter EPA MEthOd 5
Gravimetric Filter
Front EPA Method 5
Gravimetric Probe Acetone Wash
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Relinquished by:
Received by:
Relinquished by:
Received By:
Analyzed By:
Date:
Date:
Date:
Date:
Date:
Date:
Date:
f, *z -aC
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Unless otherwise indicated, all samples remain in the Custody of TETCO,
) o *, , o /. a/ ,,2/c o<'a-s ./'s,
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Figure 1. Facility Schematic Representation
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calibrationoftheconsoledrygasmeter(s),pitottubes,nozzlesdiameters,andtemperature
sensors were carried out in accordance with tire procedures outlined in the euarity Assurance
Handbook.Theappropriatecalibrationautuu,.p,.,"n..dinthefollowingpages.Thenozzle
calibrations are recotde; on the first page ofthe field data sheets'
Figure 2' Schematic of Metho d 51202 Sampling Train
Meter Box Calibration Data and Calculations Forms
Post-test Dry Gas Meter Calibration Data Forms
TYPe S Pitot Tube InsPection Data
Sample Box Temperature Sensor Calibration
Filtei Balance Calibration
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TemPerature Temperature
Difference
cr)Unit ID ThermocouPle
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(ivledium)
Reference
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SiNCE HEUSSEFI NEWEIGH :r/06
Certfficste of Balance Calibration
iCertificate No.:
Department:Address: 90 East Main St.
Citylstate/Zip: Lehi, UT 84043
Contact: Dean
Manufactuidi:' -' "Dirnver Insrd;erii -*'
,Model: A250
:Identification No.
Serial Number: 8045284lReadability: 0.0001g Capacity:
Mass Standards Used for Calibration: Cal
PRE-CALIBRATION
250g
Calibration Date:
iOraer Number:
iTechnician:
rProcedure Used:)
IIl-- :'--..-, --j?" :.-----...--..
;X - Preventive Maintenance:
iX - Calibration:
iX - Certification:
; CorrectiveMaintenance:
i Order (See Comments):
l
00657
January 12,2006
Mark B.
WP-703 @ev.2002-1)
January 12,2007
I.D. #45, Cal LD. #46,CalI.D.#47
POST-CALIBRATION
NominalMass
Value
lndicated
Weight (s)Correction (g)lndicated
Weight (g)Correction (g)3ontrol Limit +r
(s)
Post-Cal.
Within Gontrol
Limit?
1 0.99S9 -0.0001 1.0001 0.0001 0.0005 Yes
10 9.9997 .0.0003 o.0005 Yes
20 20.0001 0.0001 0.0005 YeS
50 49.9992 -0.0008 49.9995 -0.0005 0.0005 Yes
100 99.9996 -0.0004 1 00.0002 0.0002 0.0010 Yes
200 199.9985 -0.0015 1 99.9998 -0.0002 o.0020 Yes
Gomments:
Pertinent lnformation:
The mass reference standards used to calibrate and certiff this mass measurement instrument are traceable to the National
Institute of Standards & Technology (NIST) with an uncertainty less than or equal to % ofthe class tolerance. The procedure
used to calibrate the herein described artifact and this Certificate of Balance Calibration meets the requirements and guidelines
of ISO 9001:2000, ISO Guide 25, ANSINCSL 2540-l-1994, the Heusser Neweigh Quahf Assurance Program (Revision 2002'
This is to certifi the data reported herein is true and correct at the time of calibration/certification.
HEUSSER NEWEIGH 1247 West Meadorvbrook Lane, Lehi, UT 84043, [phone]
This Certificate ofCalibration shall not be reproduced except in full, without the written approval ol Heusser Neweigh.
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APPENDIX F
The testing protocol and other correspondence related to the tests are included here'
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COMPLIANCE EMISSION TESTING PROTOCOL
FOR PM1O AND CONDENSIBLE PARTICULATE MATTER AT
INTERNATIONAL URANIUM (USA) CORPORATION
BLANDING, UTAH
YELLOW CAKE NORTH DR\'ER SCRUBBER
Nday 19,2006
Project Organization and Responsibility
The following personnel and the testing contractor are presently anticipated to be
involved in the testing program. The Utah Department of Environmental euality, Division ofAir Quality (DAQ) and EPA may have their own personnel to observe all phases including the
process.
Company
lnternational Uranium (USA) Corporation
P.O. Box 809
Blanding, Utah 845i I
TETCO
90 East Main
Lehi, Utah 84043
Contacts
WallyBrice 435-678-2221
Dean Kitchen
Paul R. Kitchen
801-768-A973
Facility and Location
lnternational Uranium's White Mesa Mill is located 6 mile south of Blanding, Utah on
Highway 191. The Mill processes uranium ore. There are two yellow cake dryers with
individual scrubbers but only the Yellow Cake North Dryer is currently in operation and will be
tested.
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Test Objective
This test will be conducted to demonstrate compliance with the facility's Approval Order
No. DAeE -884-97 on the scrubber that serves the Yellow Cake ore processing operation at the
facility. Testing procedures will include accumulating process and production data as well as
testing for pM,o particulate matter emissions using EPA Method 5, with all captured matter
countld as plv1.o. Condensible particulate matter (CPM) will be measured according to EPA
Method 202 andis not for compliance but informational purposes only'
Test Schedule
it is planned to complete this testing project the week of June 26,2006.
Site Access
The sample site is located on the building
building.
Potential Hazards
Moving EquiPment - Yes
Hot EquiPment - Yes
Chemical - Yes
Other - Radioactive
roofand is accessed by stairs inside the
Process Data
All operational and instrumentation data will be made available to DAQ personnel. The
facility will run at normal conditions.
Oualit-v Assurance
All testing and analysis in these tests will be conducted according to EPA Methods 5 and
202.
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Reporting
Reporting will be prepared by the testing contractor according to EPA Quality Assurance
Guidelines. A complete copy of raw data and test calculations summary will be included in the
reports. All process and production data will be recorded by International Uranium (USA)
personnel for inspection by DAQ and EPA, if requested.
Test Procedures
Particulate matter testing will be conducted on the scrubber exhaust stack according to
EpA Method 5 . The reason for using EPA Method 5 instead of Method 20lafot PM,o is
because there are water droplets in the stack exhaust. The back-half of the Method 5 sampling
train will be sampled according to EPA Method 202 as specified in 40 CFR Part 51 Appendix M.
Method 202 isnot for compliance but for informational purposes only. Specific procedures are
as follows:
1. The sample locations and the number of sample points will comply with the requirements
of EPA Method 1.
The inside diameter of the Yellow Cake North Dryer Scrubber stack exhaust is 18 inches.
The ports are located 114 inches (6.3 diameters) upstream from the next disturbance and
114 inches (6.3 diameters) downstream from the last disturbance.
EPA Method 2 will be used to determine the gas stream velocity. T14pe "S" pitot tubes
will be used with a Co factor of 0.84. Dual inclined/vertical manometers with graduations
of 0.01 inches of water will be used. If the flows are below .25 inches of water a more
sensitive manometer will be used. The graduation marks on it are .005 inches of water.
Direction of gas flow will be checked for gas cyclonics prior to testing. If the average
deviation is over 20 degrees, then straightening vanes will be installed or other
arrangements agreeable to DAQ will be made'
Test run time will be at least 60 minutes for the Method 5 tests.
EpA Method 3 will be used to determine the gas stream dry molecular weight if the
exhaust gas is not ambient. An integrated flue gas sample will be taken from the exhaust
line after the dry gas meter orifice during each test run and analyzed at the completion of
the test with an Orsat to determine the molecular weight of the effluent gas stream' If the
exhaust gas is ambient air then TETCO will use a dry molecular weight of 28.84 lb/lbmol
(20.9 percent O.,, 79.1percent Nr) in all calculations'
EpA Method 4 will be followed to determine the gas stream moisture content.
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10.
11.
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7.
Probe liners will be 316 stainless steel for all Method 5 tests.
The back-half, or condensible particulate matter will be handled according to EPA
Method 202 andwill be for informational purposes only.
The glass fiber filters used will meet the requirements of EPA Method 5.
The barometric pressure will be measured with a barometer which is periodically checked
against a mercury barometer. The barometer will be checked prior to testing to assure an
accurate barometric pressure.
All current calibration data is submitted with this protocol, except nozzle calibration
which will be done at the test site. Nozzle calibration will be included on the first page of
each set of run sheets for each respective test run. Any calibration that is not current will
be re-calibrated prior to the test dates.
Any necessary preparation and clean-up by the contractor will be performed in the
contractor's sampling trailer or a clean area on lnternational Uranium's property. The
laboratory work and analysis will be done by the contractor as soon as possible after the
test project at 90 East Main, Lehi, Utah.
Verbal results will be reported to Wally Brice of lntemational Uranium (USA). The
written report will follow within 30 days following the completion of the test.
If maintenance or operating problems arise during the test, the test may be stopped. This
determination will be made by Intemational Uranium (USA) representatives and
operating personnel in consultation with DAQ representatives
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Estimates of Test Parameters
The values below are estimates of the stack flow rates and temperatures. These are
estimates only and are not intended to reflect permitted values.
Temperature oF
Velocity fpm
Moisture %
70
1950
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Facility Schematics
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Type S Pitot Tube Inspection Data
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Temperature Sensor Calibration
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Temperature Sqlrsor Calibration
Reference:
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PitotTube Identification: )1 - h
tecnnician: K^e -/* ^ Cor,
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Referencc:
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Dare: lZ- Z? -os--
D,
36-
h_ zfVut - ln.,^=i-.-,"
Is
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p,= Jf 4.
Pe:Ps?' t/
1.50. Dr ?- /
---fa( - \l"l
\,
c1 < 10"or=' .2 o
', oc2 < l0o
9r S5'
P:<5o Pr= I
Pr=
-.}-!
t<_-- _il:
ZsO.tZs n.( (_ lr .
w < 0.03125 in. iv: .02-/ jn.
-7--The pitot tube mcets the specifications for a calibration lactor of0.g4? ,/
z= 0L{ ? i,.
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Date:q
j
lZ-zq -os-Pitot Tubc Identification:36- >-
Technician:. R-.*-(.
D,= ? rO in.
11= 3 f/ in.
:Pe= Sf q in.
Pe: Ps ? r,/
1.50 . D. ?v
. tr;=' o. "
A,.u-
Is
Is l.05.Dr<D.<
a1 < tOo
u2 < l0'
grS5o
o,=- -l*.--.--'
Pr=
--a-
Itvv
The pitot tube meets thc specifications lor a calibration factor of O.g4? ,/
0r<5o 9t=
Z:0q in.
W < 0.03 I 25 in.w= .o r2 in.
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Date:q
lz-L-Y -o S"PitotTubeldentification: 3 d - q
Is Pn: Pr2 V'
Is 1.05 . D, < D, < 1.50 ,.Dr? {
Q",
r_l-{",a:=O"o2 < l0o
Pr 55o 0r=Oo
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b
b
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,it
\{ p,
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Jw
7= .0 o7 i".
w= .p/? i,.W < 0-03125 in.
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The pitot tube meets the specifications for a calibration factor of0.8 4? \/
Scnsor Calibration
_____+l !<_ zil
I I zs 0.125 in.rc
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Date: /) 4 O -Ofcalibraror:4 K, h/.-,ncrerencc: l/f/ Z-
Unit ID . Temperature
Difference
Cr)
Thermocouple
Location
.Temperature
Source
(l\Ierlium)
Probe Out
Probe Out
Impinger Out
Impinger Out
Probe Out
F
Oven 4-;^C7 55'
/on y',.En C/'ac,. r J
Probe Out [.t c7 6?/-- F -Zn S '. cr t€r/I
Impinger Out ,//;-69'/^6
Lrrn f .E-o,.tt:rr/
Inrpinger Out C
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SiNCE HEUS$ER F{ EWEIGH :JiO6
Certffic&te of Balunce Calibration
Calitrration Date: January 12,2446
iOrder Number:
iTechnician: Mark B.
:ProcedureUsed: WP-703 (Rev. 2002-1)
**'x
- prfi;rtil;.il6i"te"anil-- "-
lX - Calibration:
iX - Certification:
, CorrectiveMaintenance:
2509 ; Order (See Comments):
Customer Name:
Department:
Addressl
CitylStatelZip:
Contact:
TETCO
90 East Main SL
Lehi, UT 84043
Dean
Denver lnstrument
A250
Manufacturerl
ModeI:
Identification No.
Serial Number: 8045284
Readability: 0.00019 Capacity:
rv"xt caiiu;;tir;A Certification Due:January 12,2007
I.D. #45, Cal I.D. #46, Call.D. #47Mass Standards Used for Calibration: Cal
PRE-CALIBRATION POST-CALIBRATION
Gomments:
Pertinent lnformation:
The mass reference standards used to calibrate and certiff this mass measurement instrument are traceable to the National
Institute of Standards & Technology (NIST) with an uncertainty less than or equal to % of the class tolerance. The procedure
used to calibrate the herein described artifact and this Certificate of Balance Calibration meets the requirements and guidelines
of ISO 9001:2000, ISO Guide 25, ANSI/NCSL 2540-1-1994,the Heusser Neweigh Quality Assurance Program (Revision 2002'
This is to certif, the data reported herein is true and correct at the time of calibration/certification.
'1=,- la4'
Authorized Signature
HEUSSER NEWEICH 1247 West Meadorvbrook Lane, Lehi, UT 84043, [phone]
This Certificate ofCalibration shall not be reproduced except in full, without the wriften approval ofHeusserNeweigh
NominalMass
Value
lndicated
Weight (g)Correction (g)lndicated
Weight (g)Correction (g)3ontrol Limit +
(g)
Post-Cal.
Within Control
Limit?
1 0.9999 -0.0001 1.0001 0.0001 0.0005 Yes
'10 9.9997 -0.0003 o.0005 Yes
20 20.0001 0.0001 0.0005 Yes
50 49 9992 -0.0008 49.9995 -0.0005 o.0005 Yes
100 99.9996 -0.0004 100.0002 0.0002 0.0010 Yes
200 199.9985 -0.0015 199,9998 -0.0002 0.0020 Yes
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Sample Box Temperature Sensor Calibration
Datc: /) 4 ? -Oftalibrator:0 KILL.-,
Unit ID
xete,",rcc: //.t/ 7-
Temperature
Difference
cr)
C
D
Temperature
Impinger Out
Impinger Out G
Impinger Out H