DRC-2001-001022 - 0901a0688080578a

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2001
NESHAPs RADON FLUX MEASUREMENT PROGRAM
White Mesa Millsite
BIanding, Utah
Prepared for:
International Uranium (USA) Corporation
P.O. Box 809
6425 South Hwy 191
Blanding, Utah
Prepared by:
Tellco Environmental, LLC
1231N.23 St., Ste.206
Grand Junction, Colorado 81501
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Table of Contents
i.O INTRODUCTION
2.0 SITE DESCRIPTION
3.0 SAMPLER DESCRIPTION
4.0 FIELD OPERATIONS
4.1 General Site Specific Information
4.2 Sampler Placement
4.3 Sampler Retrieval
4.4 Site Exit
4.5 Enviro,mental conditions During Measurement periods
5.0 LABORATORY OPERATIONS
5.1 lntroduction
5.2 Apparatus
5.3 Analysis Procedure
5.4 Weighing and Background Counting
5.5 Receipt and Weighing of Exposed Charcoal
5.6 Gamma Ray Counting
5.7 Quality Control Samples
5.8 Data Validation
5.9 Map Preparation
5.10 Calculations
6.0 SAMPLE RESULTS/CALCULATIONS
Figure 1, Large Area Activated Charcoal Collector Diagram
APPENDICES:
A - Support Documents
B - Recount Data
C - Radon Flux Sample Laboratory Data and Blank Data
D - Figure 2, Sample Locations Map and Table I
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NES}IAPs RADON FLIIX MEASUREMENT PROGRAM
lntemational Uranium (USA) Corporation
P. O. Box 809
6425 South Hwy 191
Blanding, Utah
INTRODUCTION
During June 2001, Tellco Environmental, L.L.C. (Tellco) of Grand Junction, Colorado, provided support
to International Uranium (USA) Corporation (IUC) regarding the required National Emission Standards
for Hazardous Air Pollutants QIIESHAPs) Radon Flux Measurements effort on Tailings Cells 2 and 3 at the
White Mesa Mill uranium processing facility in Blanding, Utah. These measurements are required of IUC
to show compliance with 40 Code of Federal Regulations, Part 61, Subpart W, National Emission
Standards for Radon Emissions from Operating Mill Tailings. At present, there are no Subpart T uranium
mill tailings at this site. The regulations limit the amount of radon that can be emitted per unit area (m2)
per unit of time (s). This standard is not an average per facility, but is an average per radon source.
According to subsection 61.252 Standard, (a)radon-222 emissions to ambient air flom an existing uranium
mill tailings pile shall not exceed 20 pCtlm7-s of rudon-222. Subsection 61 .253, Determining Compliance,
states that "Compliance with the emission standard in this subpart shall be determined annually through
the use of Method 115 of Appendix 8."
Tellco was contracted to perform the on-site placement and retrieval of the radon collector canisters, as
well as the subsequent lab analysis and reporting for calendar year 2001. This report addresses the
procedures employed by Tellco and IUC to obtain the results presented in Section 6.0 of this report.
2.0 SiTE DESCRIPTION
The White Mesa Mill is located south of Blanding, Utah on Highway 191. The mill began operations in
1 980 for the purpose of extracting uranium and vanadium from feed stocks. Processing effluents from the
operation are deposited in four "lined" cells, which vary in depth. Cells I and 4 are used solely for "liquor"
storage, while Cells 2 and3 are used for sand tailings/liquor deposition.
Cell 2 has a total area of approximately 270,624 square meters (m2). This cell was comprised of two
source regions that required NESHAPs radon monitoring: approximately 246,157 m2 of the cell had a soil
cover of varying thickness, with approximately 23,867 m2 of exposed tailings "beaches". There was no
significant standing liquid in "low" elevation areas within Cell2.
Cell 3 has a total area of 288,858 m2. This cell was comprised of two source regions that required
NESHAPs radon monitoring: approximately 104,843 m2 of the cell had a soil cover of varying thickness,
with approximately 63,995 m2 of exposed tailings "beaches". The remaining approximately 120,A20 mz
was covered by standing liquid in "low" elevation areas.
Due to worker health and safety concerns expressed by both IUC site personnel and Tellco monitoring
stafl a small portion of the areas of the wet beaches of Cell 3 were not sampled due to the extreme
instability of wet tailings beaches.
3.0 SAMPLER DESCRIPTION
The Large Area Activated Charcoal Canisters (LAACC) used to perform the required radon measurements
were fabricated in confornance with "Radon Flux Measurements on Gardinier and Royster Phosphogyp-
sum Piles near Tampa and Mulberry, Florida" OITIS Document #PB86-161874) as referenced in 40 CFR,
Part 61, Method 115, Appendix B. This method of performing radon flux measurements involves the
adsorption ofradon on activated charcoal in a large-area collector. The charged collector is placed directly
on the material surface to be measured and is allowed to collect radon for a given time period (24 hours).
The radon collected on the activated charcoal is then measured by means of gamma spectroscopy.
Each LAACC was constructed using a 1O-inch PVC cap, a distribution grid that is situated on top of a lY,
inch thick layer of foam and secured under a %inch foam layer and a galvanized steel screen by a retaining
ring (see Figure 1).
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lO-in. dia
PVC End Cap
ftCURE I Large-Area Radon Col'lector
FiGURE 1
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Prior to deployment, each collector was charged with 180 grams of baked charcoal from sealed individual
sample containers (reference Section 5.0 below for laboratory procedures). After the Z4-hour exposure
period, the charcoal was transferred to the plastic sample containers, sealed with tape, labeled as to sample
identification along with exposure times/dates, and transfened to the Tellco laboratory (Grand Junction,
Colorado) facility for analysis.
4.0
4.1
FIELD OPERATIONS
General Site Specific Information
The sampling effort commenced on September 2,2001. Tellco personnel laid out baselines within the
cover regions of Cells 2 and 3, and a grid coordinate location system was developed to accommodate
locating the samplers in the field. Tellco personnel placed a high/low temperature thermometer, located
within the impoundment, to provide a record of ambient air temperatures, thereby assuring compliance
with the 35oF measurement criterion. A rainfall measurement gauge installed within the impoundment
was used to monitor and measure (if any) rainfall occurrences (see Section 4.5 for site atmospheric
conditions).
4.2 Sampler Placement
Radon measurements were made in conformance with methods described in NTIS Document #PB86-
161874 for each 100 sample measurement set for each source region. ln addition to the 100 samples, each
sample set consisted also contained five field blanks. The spacing distribution for each set of 100
measurements was determined by visual means and a "best fit" distribution pattern for each source region.
Tellco personnel identified the approximate locations of each collector to generate a sample locations map
depicting the locations of the collectors (see attached Figure 2). Vehicles were used, where appropriate,
during placement on cover material, while the placement on tailings "beaches" was accomplished by foot
travel due to safety concerns.
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Sample collection is initiated by placing 180 grams of unexposed charcoal from a sealed container into the
above described canister. A pre-measured, unexposed container of charcoal was selected from a batch,
opened and distributed evenly across the area of the support gnd. The collector was then re-assembled and
gently placed face down on the surface to be measured. Care was exercised not to "push" the device into
the soil surface. The collector rim was "sealed" to the surface using a berm of local borrow material
(either tailings or soil) to reduce dilution due to air or wind currents within the collector.
A sample identification number was assigned to each collector. Sample numbers were composed using an
alpha-numeric system that began with the charcoal batch letter (i.e., A, B, C . . .) followed by a sequential
number indicating the placement (i.e., 07,02,. . .). This sample identification number was recorded on an
adhesive label and placed on the top of the collector. The sample ID, date, and time of placement were
recorded on a master data sheet for each set of measurements. The empty containers were retained for
sample retrieval upon completion of the measurement time period (approximately 24 hours)"
During the placement of the 400 charcoal flux collectors (100 per region), twenfy field blanks (five per
region) were also collected. The procedure for field blanks was to charge a collector with charcoal and
place it inside an aitight container (e.g., plastic bag) throughout the 24-hour sample time period.
4.3 Sampler Retrieval
Retrieval of the collectors followed the same general pattern as placement. The collectors (including
blanks) were disassembled and the charged charcoal was removed, pouring it from the collector into a
large funnel suspended above a sample container. The sample ID number was transferred to the sample
container, which was sealed and placed in a box for transport. The date and time of retrieval were
recorded on the same data sheet as the sample placement information.
Sample data sheets accompanied the shipment to the laboratory. Tellco personnel assured timely delivery
of the samples to the Tellco Grand Junction laboratory for prompt analysis of the charcoal samples.
(a)
(b)
(c)
(a)
(b)
(c)
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4.4 Site Exit
Upon completion of on-site activities, the field equipment was alpha
resulting from fieldwork activities. All field equipment was surveyed
and released for unrestricted use.
scanned for possible contamination
by IUC Radiation Safety personnel
4.5 Environmental Conditions Durins Measurement Periods
Referencing 40 CFR, Part 61, Subpart W, Appendix B, Method 115 - Monitoring for Radon-222
Emissions, Subsection 2.1.4 - Restrictions to Radon Flux Measurements, "the following restrictions are
placed on making radon flux measurements:
Measurements shall not be initiated within 24 hours of a rainfall.
If a rainfall occurs during the 24 hours measurement period, the measurement is
invalid if the seal around the lip of the collector has washed away or if the
collector is surrounded by water.
Measurements shall not be performed if the ambient temperatue is below 35
degrees F or ifthe ground is frozen."
Site Specific Discussion
For this measurement sampling program, rainfall did not affect measurement initiation and no
measurable rainfall occurred during the 24-hour period preceding placement of any of the LAACC
samplers at the site.
There were no measurable rainfall events during any of the 24-how sample periods after canister
placement (as indicated by the on-site rain gauge), and accordingly, none of the LAACC seals
were washed away and none of the collectors were surounded by water.
During the four 24-hotx sample-set placements, the minimum ambient air temperature recorded at
the site was 52 degrees F.
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I 5.0 LABoRAToRy opERArroNS
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5.1 Introduction
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Activated charcoal gas adsorption collectors are passive sampling devices used to determine the flux rate
I of radon-222 gas from a surface area. As previously described, and depicted in Figure l, the collectors
utilized a 10-inch diameter PVC end cap, spacer pads, screens, and a steel retainer ring.
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Radon gas is adsorbed on the contained charcoal and subsequent radioactive decay ofthe entrained radon
t results in the deposition of radioactive lead-2l4and bismuth -214 inthe canister. These radon progeny
,+: isotopes emit characteristic gamma photons, which can be detected.I
l" The original total activity of the adsorbed radon can be calculated from these garnma ray measurements
I using empirical calibration factors derived from cross-calibration of source standards containing a known
total activity of radium-226 in a geometry identical to the samples to be counted.
I 5.2 Apparatus
I ' Single- or multi-channel pulse height analysis system, Ludlum Model 2200 with a Teledyne 3,, x 3,,
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NaI(Tl) detector.
- ' Lead shielded counting well approximately 40 cm deep with 5-cm thick lead walls and a 7-cm thick
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base and 5 cm thick top.
' ' NIST traceable aqueous solution radium-226 absorbed onto 180 gmms of activated charcoal
. Ohaus Model C50l balance with 0.1 gram sensitivity.
t 5.3 Analvsis Procedure
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Inspection of the Charcoal Container
r Charcoal was received at the analytical laboratory in the sealed sample containers. Upon receipt, the
I integrity of the container was verified by visual inspection of the plastic container.
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Sample Identification Numbers
Each sample container had a unique sample identification number, which was determined in the field, and
written onto a label attached to the sample container.
Drying and Recycling
All charcoal was dried/baked before use in the field for radon flux measurements. Procedures were the
same for newly prepared charcoal and for charcoal recycled after field use. Charcoal was baked at
approximately 110 degrees C. Baking procedures were as follows:
Oven temperature set to 110 degrees C.
Charcoal placed in the oven in a metal baking tray.
Baked for a minimum of 24 hours.
' Immediately after the tray was removed from the oven, the charcoal was transferred and sealed into
clean sample containers.
5.4 Weishinq and Backsround Countins
Proper balance operation was verified daily by checking with a standard weight. The balance readout
should agree with the known standard weight to within + O.lyo.If a discrepant readout were to occur, the
balance would be re-zeroed, the check weight wiped with a soft, lint-free cloth, and re-weighed. If the
discrepancy persisted, the balance would be removed from service and tagged "Out of Seryice." For this
project, the scale conformed for each day of use (See Appendix A, Balance Operation Daily Check fo.m).
After acceptable balance checkout, each empfy container was individually placed on the balance and the
tare weight of the containerwas documented to the nearest 0.1 grams on the label. The scale was re-
zeroed with the container on the balance. Charcoal was carefully added to the container until the readout
registered 180 grams. The lid was immediately placed on the container and sealed with plastic tape. The
tape was stretched slightly while wrapping around the container. The end of the tape was folded to form a
tab for easy tape removal. The balance was checked for readout drift between each container-weighing
step.
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Ten sets of five one-minute background counts were acquired for 10% of containers selected at random to
represent the "batch"' Each sealed container was placed individually in the shielded counting well, with
the bottom of the container centered over the detector. Five one-minute background counts were then
documented for each container, and subsequently documented on the respective "Radon Flux Field Data
Sheet" for that batch. If the background counts were too high to achieve a sufficiently low sensitivity level
(Lower Level of Detection, LLD), the entire batch was labeled non-conforming and recycled through the
dryrng process.
Gamma ray counting system checkout was performed as described in Section 5.6. Observed empty
counting well background counts must fall within the average range of approximately 100 to 15g cpm (see
Appendix A, system operation performance records) using the aforementioned Ludlum/Teledyne counting
system with shielded well.
5.5 Receipt and Weiqhins of Exposed Charcoal
Containers of exposed charcoal were hand delivered to the laboratory for analysis by Tellco personnel.
The Tellco laboratory staff was responsible for weighing and inspecting the containers of exposed
charcoal, reviewing the documentation forms and entering the required documentation into data base
spreadsheets.
When the containers were received, the following items were inspected:
. Container was closed and sealed with tape.
. Container was not damaged.
. Data sheet was complete.
' Discrepancies found during the receipt inspection were documented on the data sheet.
Containers received open or damaged resulting in seal failure were considered void.
A total of 399 samples were collected from June 11 - 15, 2001 and were subsequently received at the
laboratory in good physical condition and validated. However, the charcoal from one of the collectors (C-
33, from the Cell 3 covered region) was spilled in the field during the sampling effort.
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After receipt inspections, conforming containers were weighed on a balance to the nearest 0.1 gram and
the gross weight was logged on the "Radon Flux Field Data Sheet" under the appropriate column.
5.6 Gamma Ray Counting
Source/Background Checks
The charcoal gamma ray counting system was subjected to performance checks daily when used. These
checks included background and radium-226 calibration source measurements. (Appendix A of this report
contains daily counting system performance check records.)
Sample Analysis
. The length of count time was determined by the activity of the sample being analyzed. A data quality
objective establishing a minimum accruement of 1000 counts for any given sample was followed
during sample analyses.
The sample container was placed in the counting well with the lid side up and the center on the Nal
detector and the shielded well door was set into place.
. One sample count was accrued and the mid-sample count time and date was documented on the field
data sheet.
. The sample counts were documented on the field data sheet for data reduction.
. The above steps were repeated for each exposed sample collector.
. Every tenth container counted on a given date was selected for recounting. These containers were
recounted within three days following the original analysis, as described above.
5.7 Oualiqv Control Samples
Charcoal flux measurement QC samples included the following intralaboratory analytical objectives as
required in 40 CF& Part 61, Subpart W, Appendix B, Method 115, 4.0 - Quality Assurance Procedures for
Measuring Ra-222 Flux, D.:
. recounts, llYo, and
. equipment blanks, 5ol0.
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Samples were statistically evaluated for completeness, precision, and accuracy.
5.8 Data Validation
All sample canister data were subjected to data validation protocols. The results are as follows:
Forfy recount measurements were performed by conducting replicate analyses of individual field samples.
These recount measurements comprised approximately 10%o of the total number of samples analyzed. The
precision of all recount measurements ranged from less than lo/o to 8.1% with an overall average precision
of approxima tely 3 . 5%o.
Ten equipment blanks were analyzed by measuring the radon progeny activity in samples subjected to all
aspects of the measurement process, excepting exposurc to the source region. These blank sample
measurements comprised 5% of the field samples. The results of the blank sample analyses ranged from -
0.02 to 0.11pCi/m2-s. The average blank value of 0.05 pCi/m2-s corresponds to less than l% of the
regulatory limit of 20 pCi/m2-s.
The accuracy of the field measurements was assessed by counting a laboratory control sample with known
Ra-226 content each day that field samples were analyzed. The accuracy (percent error) of these lab
control sample measurements ranged from 1.6%o lo 2.7o/o, with an arithmetic average of -0.3% (see
Appendix A).
All samples from Cell 2 (Beaches and Covered regions) were validated, representing 100% completeness
in those regions. All samples from Cell 3 Beaches region were validated, representing 100% completeness
in that region; however, one sample from the Cell 3 Covered region was spilled, representing 99o%
completeness in that region.
As presented above, actual QC data validation met the objective parameter requirements for precision,
sensitivity, accuracy, and completeness. Reference Appendix B for QC analyses results.
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5.9 Sample Map Preparation
The approximate sample locations are depicted on Figure 2 and at the end of this report. This map was
produced by Tellco.
5.10 Calculations
Radon flux rates were calculated for charcoal collection samples using calibration factors derived from
cross-calibration to sources with known total activity with identical geometry as the charcoal containers.
A yield efficiency factor was used to calculate the total activity of the sample charcoal containers.
Individual field sample result values presented were not reduced by the results of the field blank analyses.
ln practice, radon flux rates were calculated by a database computer progmm. The algorithms utilized by
the data base program were as follows:
Equation 5.1:
pci Rn-222tm".. - o.*ffi;or=5-
where: N : net sample count rate, cpm under 220-662 keV peak
Ts = sample duration, seconds
b : rnstrument calibration factor, cpm per pCi; values used:
0.1136, for M-01/D-21 and
0.1798, for M-02/D-20
d : decay time, elapsed hours between sample mid-time and count mid-time
A : area of the collector, m2
Equation 5.2:
!S"*pl.C.-.I-* - @
Error,2o = r, x Sample Concentration
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A
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(b)
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Equation 5.3:
,yn_ 2.71 +(4.65XSbI
LLU - [TsxA*b*0.5(d/cl
75l
where: 2.71
4.65
Sr
Ts
b
: constant: confidence interval factor: standard deviation ofthe background count rate: sample duration, seconds: instrument calibration factor, cpm per pCi; values used:
0.1736, for M-01/D-21 and
0.1798, forM-021D-20: decay time, elapsed hours between sample mid-time and count mid-time: area of the collector, m2
6.0 SAMPLE RESLILTS/CALCULATIONS
Referencing 40 CF& Part 61, Subpart W, Appendix B, Method ll5 - Monitoring for Radon-222
Emissions, Subsection 2.1.1 - Calculations, "the mean radon flux for each region of the pile and for the
total pile shall be calculated and reported as follows:
The individual radon flux calculations shall be made as provided in Appendix A EPA
86(l). The mean radon flux for each region of the pile shall be calculated by summing all
individual flux measurements for the region and dividing by the total number of flux
measurements for the region.
The mean radon flux for the total uranium mill tailings pile shall be calculated as follows:
r : JlAr+...J2A2[+l...JjAiJs At
Where: J. : Mean flux for the total pile (pCi/mz-s)
Ji : Mean flux measured in region i (pCi/m2-s)
A; = Area of region i (m2)
A1 = Total area of the pile (m2)
2.1.8 Reporting. The results of individual flux measurements, the approximate locations
on the pile, and the mean radon flux for each region and the mean radon flux for the total
stack [pile] shall be included in the emission test report. Any condition or unusual event
that occurred during the measurements that could significantly affect the results should be
reported."
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' Site Specific Sample Results (reference Figure 2 and Appendix C)I
(a) The mean radon flux for each region within each cell is as follows:
Cell 2 - Cover Area : 18.2 pCi/m2-s (based on 246,7 57 m2 area)
- Beach Areas : 32.2pCilm2-s (based on23,867 m2 area)
I ""'_J#ff* Ji:1"'*;*ff::::::ff1',Jff'
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- Standing Liquid Areas : 0 pCi/m2-s (based on 120,020 m2 area)
' Note: Reference Appendix B of this report for entire summary for individual measurement
I results and specific sample region maps.
t @) Using the data presented above, we have calculated the total mean radon flux for each pile (cell) as
follows:
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Cell2: l9.4pCilm2-sI w
Cell3:10.7pCilm2-s
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APPENDIX A
Support Documents
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'
"ALAN.E
oPERArtoN DATLY cHEcK
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Barance Moder: Q ltor'n: M'blol C;o t s' ll ' tz3ol
Standard Weight (g): 2-O O
Date Pre-check (g)Post-check (g)o.K.r0.1%?By
bf,elol '7-oO.o -2-c o, o \/ rs
1pltqlot 7 0a.o '2-oo . o .) €5 >L (;>o-
blz-o /o t
"2 oa -O '7-oO.O v o->>/ 4)V*
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CHARCOAL CANISTER ANALYSIS SYSTEM
srrEl-ocArroN, V( h,tr Mrso l.di\\ , R\andi r.-q , tt+a t
CLIENT: \ ntt,;'rra\lr.]'-\r. I t^\ra!^i"d-'n lc>nf\'
Calibration Check Log
Systemp il-Ot/D-Zt CahbrationDate: 4l-z:lOl Dwoate: 4l-zifC'z.-_-r_
ScaterSA{: qt51z- (fa-c\ Highvoltage: \lOO window: 4,42 Thrshld: 2.20 -
DetectorSAr, D4l53a f D- 2) SourceID/SN,Rr""/G3-o4 SourceActivity: 59.3 (16l
2o- lCtl to t57 zo: 8, to t1 I
zo: I Cl 40 6 tolL) 3 o- r Oo5 8 b iO b53
Blank Canister Bkgd. Range, cpm:
Cross Source Range. cpm:
Technician:
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Y,Otr: Y: average background and source cpm fal1s within the conhol iimits.
N = average background and source cpm does not fall within the controi limits.
The acceptable ranges were determined from prior background and source check data
All counts times are one minute.
Date By Background Counts (1 min. each)Source Counts (1 min. each)ok?
Y/N#1 #3 Avg.#1 #2 #3 Average
Qlrblar Vk-r'L\i3 i,t t1 tz>i0+bl rD{3-l t o 4t4Q t eSos Y'oltel a wlo.2^t r20 t37 t'/-Y\t o1<o r n444 tt)4iz t2,<C)4-
b ltq lo D/,<-30 tz+t1{tvo o-t i{4 tobuln tD104 r O'7oS /v
/;/iqlo I )Lt AZ It,tzl -t-1 I O'r /l<i o b'$4 lD("11 t ObW)17
ri/zo/o DLT.Ir*io,t74-t4-i o-zz1 tO">rh tDLiq r)'>iZ-O
6lzo/o D/-L i7 ity t30 i )_l CI-L+>lO:zt I O')-1,), ()'2-2O ,Y
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CHARCOAL CANISTER ANALYSIS SYSTEM
srrElocArroN, wh',i< N\y.rr M"i{ , Bla,nii".$,ut*aL
,r1uy1-1. i n*t r^ n n*i*, 4 L V,r an'iu,n Co rf ,
System ID:
Scaler SA',1:
Calibration Check Los
lA-or /'D - I Calibration gu1"- 4lzS I O I gu"pu1", 4 {'-{f cz-
5 t s12- Cr-i- or)High Voltage: I tOC Window: 4.42 Thrshld: 2.20 -
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Detector sn{' O 4 r -5 33 LD- z\) Source ID/SN , ?o32*/ G3- oSsource Activitv , 51'l f fC
BlankCanisterBkgd.Range,cpm: 2o= [ol b 151 :o: Bl to 11 I
Y,Di: Y : average background and source cpm falls within the control limits.
N : average background and source cpm does not fall within the control limits.
The acceptable ranges were determined from prior background and source check data.
GrossSourceRange,cpm: 2r- tCte'-7 b i Cbo3 3o- lCo82- b i')ao8;
Technician: V'i 4
A11 counts times are one mtnute
Date By Background Counts (1 min. each)Source Counts (1 min. each)ok?
Y/N#1 #3 Avg.#1 #3 Average
(clrg/ ol D/./i2- \\3 in rl-l l'La ).-3r'Jl LC71)tD') I I rr3ss
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CIIARCOAL CANISTER ANALYSIS SYSTEM
sirElocA,o W h', {e irA.tsa. A"\\, B tan d j"g
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System W, Y\- oz- f D-'z-o calibrationDate:4lz< I o t DueDate: *lz5 lo'z-
ScaterSN: 5i5 Qr-l Lyi- o-D uietrvoltage: 7 5C window: 4.42 Thrshid: 2.20 -
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Technician:
A11 counts times are one minute.
YN: Y : average background and source cpm falls within the control limits.
N : average background and source cpm does not fall within the control limits.
The acceptable Ianges were determined from prior background and source check data.
Date By Background Counts ( 1 min. each)Source Counts (1 min. each)ok?
YN#1 #2 #3 Avg.#1 #3 Average
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Systemro, M-oZ /D-Z-f)Calibration oate: 4lz5l s1 9u"y16". 4lzalo z
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CHARCOAL CANISTER ANALYSIS SYSTEM
A1l counts times are one mmute.
Y,A{: Y : average background and source cpm falls within the control limits'
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The acceptable ranges were determined from prior background and source check data
Date By Background Counts (1 min' each)Source Counts (1 min. each)ok?
Y,N#1 #3 Avg.#1 #5 Average
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Figure 2, Sample Locations Map
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