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DRC-2011-002213 - 0901a06880208ec0
RC- 201 1-00 2213 DENISON MINES February 25, 2011 VIA FEDERAL EXPRESS Dsnison Mines (USA) Corp, 1050 17th Street, Suite 950 Denver, CO 8026S USA Tel : 303 628-7798 \ Fax : 303 389.4125 www.deni8onmlnes.com / Mr. Rusty Lundberg Co-Exccutivc Secretary Utah Water Quality Board Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144820 Salt Lake City, UT 84114-4820 Dear Mr. Lundberg: Re: State of Utah Radioactive Material License No. UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period JulyL 2010 through December 31, 2010 As required by Utah Administrative Code, R. 313-24-4 (incorporating by reference 10 CFR 40.65 (subpart 1)), and License Condition 11.3 A of State of Utah Radioactive Materials License No. UT 1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill for the peiiod July 1, 2010 through December 31, 2010. If you have any questions regarding this report, please contact the undersigned at (303) 389- 4132. Yours very truly. DENISON MINES (USA) CORP, Jo Ann Tischler Director, Compliance and Permitting cc Ron 1'. I loch.stcin Harold R. Roberts David C. Frydenlund David E. Turk Katherine Weinel Central I'ilcs OENISONr)~~ MINES February 25, 2011 VIA FEDERAL EXPRESS Mr. Rusty Lundberg Co-Executive Secretary Utah Water Quality Board Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144820 Salt Lake City, UT 84114-4820 Dear Mr. Lundberg: Re: State of Utah Radioactive Material License No_ UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period July1, 2010 through December 31, 2010 Denison Mines (USA) Corp. 1050 17th Stree~ Suite 950 Denver, CO 80265 USA Tel: 303628-7798 Fax : 3033894125 www.denisonmines.com As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65 (subpartl)), and License Condition 11.3 A of State of Utah Radioactive Materials License No. UT1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill for the period July 1, 2010 through December 31, 2010. If you have any questions regarding this report, please contact the undersigned at (303) 389- 4132. iL-l~ DENISON MINES (USA) CORP. Jo Ann Tischler Director, Compliance and Permitting CC Ron F. Hochstein Harold R. Roberts David C. Frydenlund David E. Turk Katherine Weinel Central Files White Mesa Uranium Mill Radioactive Materials License UT900479 Semi-Annual Effluent Monitoring Report (July through December, 2010) Prepared For: Utah Department of Environmental Quality Division of Radiation Control Prepared by Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver, CO 80265 February 25, 2011 Table of Contents 1.0 INTRODUCTION ........................................................................ , ......................... I 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING ..................................... 2 2.1 Program Overview ............................................................................................... 2 2.2 Sampling Protocol and Analytical Results ........................................................... 2 2.3 General Observations ........................................................................................... 3 2.4 Site S peci fi c Sampl ing Data ................................................................................. 4 2.5 Radon-222 ............................................................................................................ 6 3.0 EXTERNAL RADIATION (DIRECT GAMMA) .................................................. 7 4.0 VEGETATION SAMPLES ..................................................................................... 8 5 .0 STACK SAMPLING ............................................................................................... 8 6.0 SURFACE WATER MONITORING .................................................................... 10 7.0 SOIL SAMPLING ................................................................................................. II 8.0 METEOROLOGICAL MONITORING ................................................................ II 9. 0 SIGNATURE ......................................................................................................... 12 Table I Table 2 Table 3 Table 4 Table 5 Table 6 Table 7 Table 8 LIST OF TABLES NCRP Report 94-Global Pb-21 0 Concentration Example Air Monitoring Station Results U-Nat (Comparison to Limits) 2nd and 3rd Quarters 20 I 0 Air Monitoring Station Results Th-230 (Comparison to Limits) 2nd and 3rd Quarters 2010 Air Monitoring Station Results Ra-226 (Comparison to Limits) 2nd and 3rd Quarters 2010 Air Monitoring Station Results Pb-210 (Comparison to Limits) 2nd and 3rd Quarters 20 I 0 Environmental TLD Measurements (Gamma) Stack Sampling Requirements Stack Effluent Concentrations and Release Rates INDEX OF TABS A High Volume Air Monitoring Stations B BHV Air Sampling Graphs and Data Tables Tabl BHV-l Air Sampling Graphs and Data Table Tab 2 BHV-2 Air Sampling Graphs and Data Table Tab 3 BHV-3 Air Sampling Graphs and Data Table Tab 4 BHV-4 Air Sampling Graphs and Data Table Tab 5 BHV-5 Air Sampling Graphs and Data Table Tab 6 BHV-6 Air Sampling Graphs and Data Table C Air Particulate Loading Graphs and QAlQC D Air Particulate Loading Graphs and Supporting Data E Environmental Gamma (TLD) Graphs and Supporting Data F Vegetation Graphs, Data Table, Laboratory Results and QA/QC G Stack Sample Laboratory Results H Surface Water Graphs and Field Data Sheets I Soil Sample Graphs, Data Table, Laboratory Results and QA/QC 11 WHITE MESA URANIUM MILL SEMI-ANNUAL EFFLUENT REPORT, JULY THROUGH DECEMBER, 2010 1.0 INTRODUCTION The White Mesa Mill (the "Mill") has established monitoring programs to evaluate compliance with effluent limitations and to assess the potential for release of radioactive material into the local environment. These monitoring programs were developed and implemented at the time of Mill construction, operated with appropriate adaptation over time, and are consistent with the Mill's State of Utah Radioactive Materials License No. UTl900479 (the "License") and guidelines developed by the United States Nuclear Regulatory Commission ("NRC") (NRC Regulatory Guide 4.14, Radiological Ejjluent and Environmental Monitoring at Uranium Mills-Rev. ], ML003739941), 1980). Under these programs, the Mill monitors the following environmental media and conditions: a) Airborne particulate radionuclide concentrations obtained from the following sampling stations: • North, east and south of the Mill Site: BHV -I and BHV -2 (north), BHV-5 (east), and BHV-4 (south). BHV-I serves as a surrogate for the nearest resident (BHV -I is approximately 1.2 miles north of the Mill, but approximately 0.4 miles closer to the Mill than the nearest resident); • A background location distant to and west of the Mill (BHV -3), which was monitored for airborne particulate up until November, 1995, at which time background was established, but is no longer monitored for air particulate; and • A station specifically requested by the White Mesa Ute Community south ofthe Mill Site (BVH-6); a) External (direct) gamma radiation measured at air monitoring stations BHV -I , BHV-2, BHV-3, BHV-4, BHV-5 and BHV-6; b) Vegetation at three site periphery locations, for uptake of radiation; c) Stack release rates from the Mill's air emissions sources; d) Surface water at Cottonwood Creek and, when flowing, Westwater Creek, both located west of the Mill; e) Soil radionuclide activity obtained near the air particulate monitoring stations, during the third quarter of each year; N:\Rcquircd Rcports\Semi Annual Emucnt Reports\20 10 July to Dcc\Jul_lo _Dec _20 10_ Semi_ annual_ Effiucnl_Rcport_Main_lcxt.docx f) Groundwater (up and down gradient) of the Mill facility; and 1 g) Seeps and springs in the vicinity of the Mil!.l This semi-annual effluent report provides the results of the specific monitoring and sampling activities that were undertaken during the subject reporting period. 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING 2.1 Program Overview The environmental airborne particulate monitoring program at the Mill utilizes four air sampling stations. Four high-volume continuous air sampling stations (BHV -I, BHV -2 , BHV-4, and BHV-5) are required by the License. These sampling stations serve as sentinels for airborne particulate which could potentially emanate from the Mill site. In addition to its general site monitoring function, BHV -1 also serves as a conservative surrogate for concentrations at the nearest resident, because it is located approximately 1.2 miles north of the Mill just south of the nearest resident but between the Mill and that resident. With regard to background monitoring, the Mill previously operated a continuous high- volume air sampling station (BHV-3) which was located approximately 3.5 miles west of the Mill site. With the approval of NRC, this station (BHV-3) was removed from the active air monitoring program in November 1995. At that time, NRC determined that a sufficient air monitoring data base had been compiled at BHV -3 to establish a representative airborne radionuclide background for the Mil!. It should be noted, however, that while air sampling was discontinued at this location, gamma measurements and soil sampling continue to be collected at BHV-3. In addition to the environmental air sampling locations described above, an additional station (BHV -6) was installed at the request of the White Mesa Ute Community. This station began operation in July of 1999 and provides airborne particulate information in the southerly direction between the Mill and the White Mesa Ute Community 2.2 Sampling Protocol and Analytical Results Airborne particulate monitors are operated continuously at each of the high-volume air sampling stations referenced above. Particulate sample collection filters are gathered by site technicians weekly in accordance with the Mill's environmental air sampling procedures and are composited on a quarterly basis for laboratory analyses. The collected filters are analyzed for Unat activity, Th-230 activity, Ra-226 activity, and Pb- 210 activity. Fugitive dust standards for the facility are limited by the Mill 's State of I Groundwater sampling and seeps and springs sampling are reported separately pursuant to the Mill's State of Utah Ground Water Discharge Permit No. UGW370004, and is not included with this report. 2 N:\Requircd Rcports\Semi Annual Effiucnt Reports\2010 July to DccVuUo _Dec _ 20 10_ Scmi_ annual_Effluent_Report _Main_tcxt.docx Utah Air Approval Order, which sets a 20% visual opacity standard. The specific locations of the Mill's airborne particulate monitoring stations are depicted on the figure entitled High Volume Air Monitoring Stations included as Attachment A. Station BHV- 3, which is no longer sampled for air particulate is located approximately 3.5 miles west of the Mill facility and is not indicated on that Figure. The analytical results of radionuclide particulate sampling for each monitoring station operated during this July through December, 2010 reporting period are provided in Attachment B under separate sampling station attachment tabs (Tabs 1-6). Each Tab contains graphical illustrations of the radionuclide concentrations in log-scale presentation format. The graphs display reported data over time since the 1981 inception of the Mill's environmental air particulate monitoring program. The actual analytical results (and associated QA/QC information) reported by the laboratory are provided under Attachment C. In addition to the analyses for radionuclides, particulate loading is determined for each filter and composited as a quarterly mass-loading estimate for review purposes only. Graphs showing particulate loading at each station for the second half of 2010 and the underlying data are included as Attachment D. It should be noted that for graphical illustration purposes, values reported at zero, values reported at less than the Ptrescribed detection limit « 1 x 10-16 uCi/ml) and missing values were plotted as 1 x 10-6 uCi/ml concentrations. Where other "less than" values were indicated (i.e., where detection limits for the data varied from 1 x 10-16 uCi/ml), the detection limit concentration was utilized for plotting the data point. This graphing convention is not utilized to formulate station average information, nor is it intended as a precedent for data treatment. Rather, the intent is to provide a conservative viewable depiction of site airborne radionuclide information. This is considered to be a conservative approach because the actual concentration below the detection limit cannot be determined and, as a result, the plotted point will be at the same or a higher concentration than the actual activity concentration of the collected sample. 2.3 General Observations The results of environmental air monitoring for this semi-annual period indicate that for all radionuclides at all monitoring stations airborne radionuclide particulate activity concentrations were well below regulatory Effluent Concentration Limits ("ECL's") and the Mill's ALARA goals, which are set at 25% of the ECLs. It is noteworthy and expected that Pb-21 0 concentrations are elevated when compared to the other parent radionuclide concentrations (i.e. U-nat, Th-230 and Ra-226). This phenomenon is due to the well-established controlling effect experienced worldwide as a result of the ubiquitous presence of radon in the earth's atmosphere. Accordingly, elevated Pb-21 0 presence in disequilibrium with parent radionuclides measured here is not associated with uranium milling operations. Rn-222 emanates as a decay-chain progeny of the Ra-226 contained in the soil of the earth's crust and is dispersed generally throughout the earth's atmosphere. The electrically charged short and long-lived decay 3 N:\Rcquired Rcports\Semi Annual Effluent Reports\2010 July to DecVul_ to_Dec _20 10_ Semi _ annuaJ_ Emucnt_ RcpoI1_Main_texLdocx products of Rn-222 attach to ambient dust particles found naturally in the atmosphere and are carried with the air. Pb-21 0 is the longest lived of these decay products and is the decay product ofthe shorter-lived radon progeny. As such, it accumulates as an electrical attachment on the natural ambient dust in the atmosphere and is generally measured at elevated activity when compared to local decay-chain parent radionuclide activity, regardless of uranium milling activity. At the Mill's BHV air monitoring stations, all dust (ambient natural and mill derived) is collected by the sample filter. Because of the natural elevation of Pb-2l0 accumulated as an attachment to the naturally occurring ambient dust particles collected by the air sampling equipment, Pb-210 is commonly elevated and in disequilibrium when compared to parent radionuclide activity, regardless of the Mill's presence. By way of illustration, average ground-level concentrations have been reported for selected States (NCRP Report 94, 1992) and are summarized in Table I below, demonstrating elevated Pb-210 activity where no uranium milling operations are located nearby. Pb-210 activity concentrations can be expected to be even higher for locations in the western U.S. where uranium ore bodies are commonly located. In April 1977, prior to Mill construction and Mill operations, air particulate Pb-21 0 was measured at the Mill site to be I.3E-14 uCi/ml (13.0E-3 pCi/m3)2 Table 1-NCRP Report 94-Global Pb-210 Concentration Example State Pb-210 Concentration uBqlM' uCi/ml California 600 1.6E-14 Illinois 1500 4.IE-14 Ohio 300 8.IE-IS Massachusetts 700 1.9E-14 2.4 Site Specific Sampling Data The results of airborne particulate monitoring for the period (without background subtraction) are provided by sampling station and radionuclide in Tables 2 through 5 below. Along with these data, the tables present comparative ECL's and the ECL percentage measured at each of the monitoring stations sampled during the period. A review of these data supports the conclusion that airborne particulate is well controlled at the Mill. In all cases, the measured activity concentrations were well within the ECL, as well as the Mill 's ALARA goal (i.e. 25% of the ECL). It should also be noted that the analytical laboratory maintained Lower Limits of Detection consistent with NRC Regulatory Guide 4.14 for this reporting period. In fact, the data obtained since program inception in 1981 indicates that only one individual quarterly measurement (Th-230 at BHV -5 for the 2nd Quarter of 1996) has 2 See the Environmental Report. White Mesa Uranium Project. San Juan County, Utah for Energy Fuels Nuclear, Inc. prepared by Dames & Moore, January 30, 1978, Section 2.9.1.1 4 N:\Rcquircd Reports\Semi Annual Effiuent Reports\20 10 July to Occ\JuUo_Dcc_2010_Semi_annual_Effiucnt_Rcport_Main_tcxLdocx ever exceeded the ECL at the Mill. With regard to that particular single measurement, while it is important to consider and evaluate an individual measurement exceeding the ECL, for public dose estimation purposes it is the average annual concentration that is of primary significance. In that instance, the average annual concentration of Th-230 for BHV -5 in 1996 was well below the ECL. Data obtained since program inception in 1981 also indicate that, with very few exceptions, the gross (background inclusive) measurements do not exceed the site's ALARA goal (i.e. only nine of the several thousand total gross radionuclide determinations to date exceeded the Mill's self-imposed 25% ALARA goal). Table 2-Air Monitoring Station Results U-Nat (Comparison to Limits) 3rd and 4th Quarters 2010 Monitoring 3"' Qtr. 4'h Qtr. Effluent Average Station Result Result Concentration Percent (uCi/ml) (uCi/ml) Limit (ECL) ECL (uCi/ml) BHV-1 8.42E-16 I.27E-15 9 E-14 1.17E+00 BHV-2 2.91E-16 5.73E-16 9 E-14 4.80E-Ol BHV-4 4.77E-15 3.93E-15 9 E-14 4.83E+00 BHV-5 3.57E-15 8.52E-15 9 E-14 6.72E+00 BHV-6 5.42E-15 1.24E-14 9 E-14 9.90E+00 Table 3-Air Monitoring Station Results Th-230 (Comparison to Limits) 3rd and 4th Quarters 2010 Monitoring 3'd Qtr. 4°' Qtr. Station Result Result (uCi/ml) (uCi/ml) BHV-I 2.80E-16 2.32E-16 BHV-2 4.48E-17 7.24E-17 BHV-4 1.80E-15 3.90E-16 BHV-5 1.14E-15 1.45E-15 BHV-6 1.08E-15 1.21E-15 5 N:\Requircd Reports\Semi Annual Effiu ent Reports\2010 July to Dcc\JuUo _Dec _201 0_ Scmi_ annual_ Effiuenl_ Report_Main _ tcxt.docx Effluent Average Concentration Percent Limit (ECL) ECL (uei/ml) 2 E-14 1.28E+00 2 E-14 2.93E-Ol 2 E-14 5.48E+00 2 E-14 6.48E+00 2 E-14 5.73E+00 Table 4-Air Monitoring Station Results Ra-226 (Comparison to Limits) 3rd and 4th Quarters 2010 Monitoring 3nl Qtr. 4°' Qtr. Effluent Average Station Result Result Concentration Percent (uCi/ml) (uCi/ml) Limit (ECL) ECL (uCi/m!) BHV-I I.3IE-16 2.30E-16 9 E-13 2.0IE-02 BHV-2 5.72E-17 6.76E-17 9 E-13 6.93E-03 BHV-4 8.23E-16 2.56E-16 9 E-13 5.99E-02 BHV-5 7.97E-16 1.29E-15 9 E-13 1.16E-OI BHV-6 5.68E-16 1.00E-15 9 E-13 8.7IE-02 Table 5-Air Monitoring Station Results Pb-210 (Comparison to Limits) 3rd and 4th Quarters 2010 Monitoring 3nl Qtr. 4th Qtr. Effluent Average Station Result Result Concentration Percent (uei/ml) (uCi/ml) Limit (ECL) ECL (uCi/ml) BHV-I 6.80E-15 1.27E-14 6 E-13 1.63E+00 BHV-2 1.08E-15 1.35E-14 6 E-13 1.22E+00 BHV-4 5.IIE-15 1.13E-14 6 E-13 1.37E+00 BHV-5 3.78E-15 1.33E-14 6 E-13 1.42E+00 BHV-6 3.98E-15 1.53E-14 6 E-13 1.61E+00 2.5 Radon-222 Due to the unavailability of monitoring equipment to detect the new 10 CFR Part 20 standard, and with the approval of NRC, Radon 222 monitoring at BHV stations was discontinued in 1995 . Instead, Denison demonstrates compliance with these limits and the requirements of R313-15-30 I by calculation, authorized by the NRC and as contemplated by R313-15-302(2)(a). A copy of the Technical Evaluation Report evidencing such approval was enclosed with correspondence to the Division on July 28, 2008. This calculation is performed by use of the MILDOS code for estimating environmental radiation doses for uranium recovery operations (Strenge and Bender 1981) and more recently in 2003 by use of the updated MILDOS AREA code (Argonne 1998). The analysis under both the MILDOS and MILDOS AREA codes assumes the Mill to be processing high grade Arizona Strip ores at full capacity, and calculates the 6 N:\Rcquircd Rcports\Scmi Annual Emucnt Rcports\2010 July to Dcc\JuUo _Dec _20 10_ Scmi_annual_Emucnt_ Rcpol1_ Main _ tcxt .docx concentrations of radioactive dust and radon at individual receptor locations around the Mill. The MILDOS and MILDOS AREA codes calculate the combined Total Effective Dose Equivalent ("TEDE") from all relevant pathways, including both air particulate and radon, at a number of locations including the nearest residence (the individual likely to receive the highest dose from the licensed operation), approximately 1.6 miles north of the Mill. These calculations reveal projected doses to the individual likely to receive the highest dose from the licensed operations to be well below the 1 00 mrem regulatory limit in R313-15-301(1)(a) for all pathways, including air particulate and radon, and well below the ALARA goal of 10 mremlyr for air emissions excluding radon as set out in R313-15-1 01 (4). MILDOS AREA modeling was recently conducted in support of the Mill's 2007 License Renewal Application, utilizing the MILDOS-AREA code (Version 2.20~), to estimate the dose commitments at various receptor locations for processing of Colorado Plateau ore (0.25% U30 g and 1.5% V 205) and Arizona Strip ore (0.637% U30 g). The process rate was assumed to be at full capacity of 730,000 tons per year (an average of 2,000 tons per day) with an average uranium recovery yield of 94%. That modeling showed a TED E of 2 mrem per year at the nearest resident (3 mrem per year at the nearest potential residence, being the location of BHV -I at the northern property boundary of the Mill site), which included the dose from all radionuclide sources, including radon. The modeled dose from radon itself was therefore a fraction of TEDE and well within the regulatory limits. 3.0 EXTERNAL RADIATION (DIRECT GAMMA) Gamma exposure rate estimates were measured for the 1st and 2nd quarters of 2010 utilizing passive integrating devices, thermo luminescent dosimeters ("TLD's"). These dosimeters were located at each of the Mill's high-volume air sampling stations (BHV-I, BHV-2, BHV-4, BHV-5 and BHV-6) and at the designated background monitoring station (BHV-3). Measurements obtained from location BHV-3 have been designated as background due to BHV-3's remoteness from the Mill site (i.e. BHV-3 is located approximately 3.5 miles west of the Mill site). The results of the environmental TLD measurements and semi-annual cumulative above-background data are provided in Table 6 below. In addition, measurement data obtained at these locations are graphically presented at Attachment E to this report. 7 N:\Requircd Rcports\Semi Annual Effiuent Rcpol1s\2010 July to OccVul_to_Dcc_2010_Scmi_annual_Efflucnt_Repol1_Main_tcxLdoex Table 6-Environmental TLD Measurements (Gamma) Monitoring 3'· Qtr 4th Qtr 3"' Qtr 4th Qtr Cumulative Station Result Result Result Less Result Less Semi- (rnrem) (rnrem) Background Background Annual (rnrem) (rnrem) Estimate* (rnrem) BHV-I 29 35.5 7.4 4.4 11.8 BHV-2 24.8 36.7 3.2 5.6 8.8 BHV-3 21.6 31.1 0 0 0 BHV-4 20.4 34.7 -1.2 (0) 3.6 3.6 BHV-S 28.1 37 6.5 5.9 12.4 BHV-6 20.5 31.7 -1.1 0.6 0.6 *Negative values treated as zero for cumulative dose The results for this period indicate that above background measurements for stations BVH-I, BVH-2, BVH-4, BVH-S and BHV-6 are within regulatory li mits. BHV-I is at the location of the nearest potential residence. The nearest actual residence is approximately 0.4 miles north of BHV -I. The annual individual member of the public limit is 100 mremJyr for combined internal and external exposure. 4.0 VEGETATION SAMPLES Vegetation samples are collected at three locations around the Mill property. The sampling locations are: I) northeast, 2) northwest and 3) southwest of the Mill facility. The vegetation samples are collected during early spring, late spring and fall (i.e., the growing seasons). Graphical log-scale presentation of the vegetation sampling results for this reporting period, together with the analytical results reported by the Mill's contract laboratory (including QAlQC information) are included at Attachment F of this report. The 3'd quarter data results are within the variation of previous sampling episodes. 5.0 STACK SAMPLING Under Section S.O of Tab 1.4 of the Mill 's Environmental Protection Manual, Revision: DUSA-l, 2/07 (the "Environmental Protection Manual") gas stack samples are collected at the Mill in accordance with the calendar year schedule shown below: 8 N:\Rcquircd Rcports\Scmi Annual Effiuent Repolts\2010 Ju ly to DecVuUo_Dcc_2010_Scmi_annual_Effiucnt_Rcport_Maio_text.docx Table 7 -Stack Sampling Requirements Frequency Feed Stack (Grizzly Stack for Packaging 8aghouse) Yellowcake Dryer (Yellowcake 8aghouse) Quarterly None If operating, V-nat If operating, V-nat Semi-annually If operating, V-nat, If operating, V-nat, If operating, V-nat, Th-230 Th-230, Ra-226, Pb-Th-230, Ra-226, 210 Pb-21 0 The yellowcake dryer and yellowcake baghouse operated during the 3rd Quarter of2010. The yellowcake dryer, yellowcake baghouse, and grizzly operated during the 4th quarter of2010. The analytical results of stack sampling conducted for the 1st and 2nd Quarter of2010, as well as for the 3rd and 4th Quarters of20l0, are provided in Table 8 below, indicating the uCi/cc concentration in the stack emissions and the stack's radionuclide release rate (uCi/sec) for V-Nat, Th-230, Ra-226 and Pb-210 at each of the stacks sampled. The actual analytical results reported by the laboratory for the yd and 4th quarters of 201 0 are provided in Attachment G to this report. It is also important to note that stack effluent concentrations are not comparable to environmental air sampling station ECL's for regulatory compliance purposes. The ECL is a limit that applies to the receptor locations and is not applicable to effluents from mill processes on the Mill site. These stack release data are more appropriately utilized for dose modeling purposes, and dose modeling is not computed for semi-annual reporting purposes. 9 N:\Rcquircd Rcports\Scmi Annual Effluent Rcports\2010 July to DecVuUo_Dcc_2010_Semi_annual_Effiuent_Repol1_Maio_text.docx Table 8-Stack Effluent Concentrations and Release Rates V-Nat V-Nat. Th-230 Th-230 Ra-226 Ra-226 Pb-2 10 Pb-210 uCilcc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec 1ST Qtr, 2010 North YC Dryer 7.3 IE-09 4.14E-03 Not Not Not Not Not Not Scrubber, Run I required required required required required required North YC Dryer 9.94E-13 6.00E-03 Not Not Not Not Not Not Scrubber, Run 2 required required required required required required Yellowcake Baghouse 1.02E-11 l.ll E-05 Not Not Not Not Not Not required required required required required required 2"d Qtr, 20 I 0 North YC Dryer 6.22E-07 3.4IE-OI I.B9E-12 1.03E-06 1.07E-13 5.B4E-OB 1.90E-12 1.04E-06 Scrubber, Run I North YC Dryer B.23E-09 4.51 E-03 B.40E-12 4.60E-06 4.74E-14 2.60E-OB 2.66E-12 1.45E-06 Scrubber, Run 2 Yellowcake Baghouse 2.99E-IO 2.90E-04 1.5BE-12 1.53E-06 l.lBE-13 1.14E-07 3.03E-13 2.94E-07 Grizzly Baghouse 2.03E-12 1.55E-06 1.33E-13 1.02E-07 Not Not Not Not required required required required 3'd Qtr, 2010 North YC Dryer 6.97E-09 4.21 E-03 Not Not Not Not Not Not Scrubber, Run I required required required required required required North YC Dryer 9.02E-09 5.32E-03 Not Not Not Not Not Not Scrubber, Run 2 required required required required required required Yellowcake Baghouse 1.37E-09 4.57E-05 Not Not Not Not Not Not required required required required required required 4th Qtr, 2010 North YC Dryer 1.44E-OB 7.33E-03 2.IOE-II 1.07E-05 3.32E-12 1.69E-06 B.B9E-14 4.53E-OB Scrubber, Run 1 North YC Dryer 1.25E-OB 6.5 IE-03 7.97E-12 4.14E-06 2.73E-12 1.42E-06 2.IBE-13 1.13E-07 Scrubber, Run 2 Yellowcake Baghouse 1.05E-09 9.19E-04 5.50E-12 4.BOE-06 2.B7E-13 2.5 IE-07 4.23 E-14 3.69E-OB Grizzly Baghouse B.IBE-12 5. 1 OE-06 9.75E-14 6.07E-OB Not Not Not Not required required required required 6.0 SURFACE WATER MONITORING Under the License, Part 11.2 B surface water samples are required to be obtained annually from Westwater Canyon and semi-annually from Cottonwood Creek. Sediment samples from Westwater Canyon are taken in place of the Westwater Canyon surface water sample in the event that surface water is not available for sampling. Westwater Canyon surface water was sampled in the first quarter 2010 and as such no sediment sample was necessary during 2010. The surface water sample from Westwater Canyon is 10 N:\Rcquircd Rcports\Scmi Annual Emucnl Reports\20JO July to DccVuUo _Dec _20 I 0_ Semi_ annua l_ Emucnl_ Report_Main _lCx.t.docx discussed in the previous SAER dated August 31 , 2010. Under Part I of the Mill's Environmental Protection Manual, surface water samples are required to be obtained annually from Westwater Canyon and quarterly from Cottonwood Creek. The Mill's Environmental Protection Manual, requires that Cottonwood Creek be sampled for total dissolved solids (TDS) and total suspended solids (TSS) quarterly and dissolved and suspended radionuclides including Gross Alpha, Unat, Ra-226, Th-230 semi-annually. In accordance with these requirements, Cottonwood Creek was sampled for TDS and TSS both 3'd and 4th quarter and for the dissolved and suspended radionuclides noted above during the 4th quarter. Additional sampling was conducted during the 1st and 2nd Quarters 2010 as discussed in the previous SAER dated August 31 , 2010. Cottonwood Creek is an intermittent ephemeral drainage located southwest and down- gradient of the Mill complex. Westwater Canyon is a drainage located west of the Mill facility, which is rarely flowing. The field data sheets for the surface water sampling attempts, along with graphs showing historic results are included as Attachment H. 7.0 SOIL SAMPLING Under Tab 4.1 of the Mill's Environmental Protection Manual, surface soils are required to be sampled at the Mill's air monitoring stations (BHV-I , BHV-2, BHV-3, BHV-4, BHV -5 and BHV -6) once per year during August or as soon as possible thereafter, but no later than September 30 of each year. All soil samples will be analyzed, on a dry basis, for Ra-226 and U-nat. Annual soil samples were collected by the Mill staff during August 2010 at the six air monitoring stations. The results of these samplings indicate that soils at the air monitoring stations remain low and within the range of typical background. A graphical presentation of historical results for soils at the air monitoring stations, together with analytical sample results for the August 2010 sampling are provided in attachment I. 8.0 METEOROLOGICAL MONITORING As in prior reporting periods, an independent contractor has prepared the White Mesa Mill Semi-annual Meteorological Monitoring Report for the period of July through December,2010. This information is retained at the Mill site for agency review. 11 N:\Rcquircd Rcports\Scmi Annual Effluent Reports\2010 July to DeeD u1_to _Dec _20 10_ Scmi_annual_ Effiu ent_ Rcpol1_ Main _Icxl.docx 9.0 SIGNATURE This Report was prepared by Denison Mines (USA) Corp. on February 25, 2011. By: David C. Fryd Vice President, Regulatory Affairs and Counsel 12 N:\Rcquircd Reports\Semi Annual Effluent Rcports\2010 July to DccVuUo_Dcc_2010_Scmi_annual_Effiuent_Rcpot1_Main_text.docx ATTACHMENT A HIGH VOLUME AIR MONITORING STATIONS w:\USA\lJIah~edamalion Plans\Recf'lan 32·ftnal\F'lQ~s 2.3-1_ At Mcri:oriog.dwg FlQUrs 2.3-1 14~1/2011 brrunkhbaatar r \ ", .... ~' '-I .. .-J :; '~/ : ... ~ ., ....:, "II ,,', ": .. .t ,; ,-J .. " ~ l ~ ..• ' v "'" J: / l , ' ~ 1 / l i U / ! \.. --, \ -\\ " I 'S>, ~ '.\~ \ , , .. ~ o BHV-2 I I , , / , \ , N yo l ~ I I ~ , +-fl , ) 2000 ~ 0 2000 ~U SCAlE IN FEET -, -; i --, I ., _ I .. '! I , .. --, ' 6 ~ .... k ! /1 ,~,,;II f , , ( \J ... ~ .. --, --,'''' " ~ /.~ , ,'I' " ..'/ ~, ; ~ " :, , -('-" , .,.~,' ~, , I '. '\ .. ...."---, ~'A t-.. ... -' .. fit" " G~~" !fElL NO, Il f ~~ "" ~ .. , ~ .. \ .. 1J-\.flf..... ....' ........ ,/ , ... _, • .-,,,~4Ir ') l ,/' (.)' , , .. , .. / , " t--.-\ , , \ I , , \ , ... '\ .. • --f ( f'" , , --' g ,: o , i \ ~ , :Z. .. .. I --..I ." -.. ;\ ---, / \"''''''' I _,,~ --,,~,p k , , ~--" , \ '\. --I -- o BHV-4 CELL NO, 2 o BHV-5 o BHV-6 ~ :...:. J : :. .. ' I .. . " \ ,.. -/ , 1-01 A ~ , -"'\ = " j ) , .• ' j '\ , -=\" :. -~ , ... -, . ; \- "') :\ .,.,,.! ! = \.... \ i ,,\" ~ ":. #, \'.... c. I .... ',,-'... ~ .. I " , , ~ J .. ~, '" ... ~ 'to)-~\ ,-..£. , t; t", l. -"":'\ w -0 : ~·i ·0 ",-.. , '" '\~h' ~" : ',.. ..A .... , "",,",... ~ ".-., (, )' , 191 {, , , ~ ;I", "",'\ '! ,(:, 3'~ ! :1."', -." ~ I ~. .. ~ ',-' ~ , -. '" \ . ~ ~, " ''---... ;: , "< "'-"t'" '\ .. .. '\ \. , I ~ , ~. .. ~~.-. ~ tv.' ~I ~-~,; l .. ~" .-' , / \ , ---'--, '-I ( i V ';:, "\ ... "'.it 0 ~,,-.. " ,. ... VJ ~,7 ~ U" Property Boundary Reservation Boundary _"_"_ Canyon Rim .. ,. \ ", .. Ii .. oil o Air Monitor Stations I -, -~ '-.. I--'\ " " ...... t .. , .... .. .. '1-~, t~i' ,,' Denison Mines (USA) Corp. Project WHITE MESA MILL REVISIONS County: SAH JIJ.AH ocallon: Date By 11/09 dill 1/131\1 8M 1/27111 aM rSt3te: UT Figure 2,3-1 High Volume Air Monitoring Stations .. -~1 '" " •• NOSOJ)JJ MINIS fi ure 2.3-CClir ~itori"l.dwg y. B. Wunkhbaator ATTACHMENT B BHV AIR SAMPLING GRAPHS AND DATA TABLES TAB I BHV-I AIR SAMPLING GRAPHS AND DATA TABLE IDate limit: Pre 1994 MPC limit:: ~IBHV-lU uCi/ml n limit = 2E-14 uCi/mIISHV-l1 5E-13 uCi/ml 8E-14 uCi/ml limit = 9E-13 uCi/ml BHV-IR Pre 1994 MPC limit = 2E-12 uCi/ml Pre 199 Pre 1994 ALARA GOAL = .. , .. .&::>~ ...... "'" uu .... - ALARA Goal = 2.25E-13 uCi/ml tiARA Goal = 5E-13uCi/ml ---- 5 uCi/ml ISHV-IPS 14E-12 uCi/ml Cone Cone IEFC IEFCA ICone IEFC IEFCA 9/28/1981 1z.35E-15 15.ooE-12 11.25E-12T7.82E-16 18.00E-14 12.00E-14T1.06E-15 12.00E-12 5.00E-13 2.57E-14 4.00E-12 1.00E-12 12/14/1981 1.56E-15 5.ooE-12 1.25E-12 1.49E-15 18.00E-14 2.00E-14 h.93E-15 2.00E-12 5.00E-13 2.64E-14 4.00E-12 1.00E-12 "/~,,,,".-.o .. 12.16E-15 15.00E-12 11.25E-12 2.93E-15 8.00E-14 2.00E-14 1.16E-15 2.00E-12 5.00E-13 2.09E-14 4.00E-12 1.00E-lil 4.00E-12 1.00E-12 11/3/1984 12.87E-15 15.ooE-12 [1.25E-1211.14E-16 ._ }8,.oOE.:.14 b.oo~-~~ 1~:;9~-;6 !z:ooE-12 15:ooE-13 !t.06E-14 1~:OUt-1l k~t-1l 14/2/1984 11.59E-15 15.00E-12 11.25E-1213.40E-16 18.00E-14 12.ooE-1413.71E-16 12.ooE-12 15.00E-13 13.34E-14 14.ooE-12 11.00E-12 /19s4 -h.10E~15 '15.00£-12 11.25£-12 1.00E-15 2.ooE-1412.09E-15 12.00E-12 15.00£-1311.88£-14 14.ooE-12 11.00E-1: 1.25E-12 1.39E-16 8.00E-14 2.ooE-.... , ... /1985 lo.oo£-too 15.00E-12 11.25E-1211.23E-15 [8.00£-14 12.00E-~~ I~:~~-~~ 12:00~-~2 15:ooE-~318:o6~-1~ kOUE-tz k~E-1Z 17/1/1985 17.17£-16 1.05E-15 2.15E-14 1.00E-12 i.13E-16 5.00E-12 1.25E-12 1.18E-16 8.00E-14 2.00£-14 3.71E-16 3.64E·15 1.00E-1: ... -,.. 12.ooE-12 5.00E-13I 14.00E-12 11.00E-12 :.42E-15 5.00E-12 1.25E-12 4.74£-16 8.00~ - . 1986 3.98E-15 9.74E-16 2.00E-12 5.00E-l 5.51E-17 3.52E-16 !}7E-15 2.ooE-12 5.00E-13 1.23E-14 1.ooE-12 1.99E-15 5.00E-12 1.25E-12 3.06E-16 8.ooE-14 2.00E-14 1.25E-15 2.00E-12 5.00E-13 1.08E-14 4.00E-12 1.00E-12 2/15/1986 1.67E-15 5.00E-12 1.25E-12 1.16E-16 8.ooE-14 2.00E-14 5.98E-16 2.00E-12 5.00£-13 1.37E-14 4.00E-12 1.00E-12 /16/1987 2.33E-15 5.ooE-12 1.25E-12 4.3OE-16 8.00E-14 2.00E-14 1.92E·16 2.00E-12 5.00E-13 5.59E-14 4.00E-12 1.00E-12 .. --2.36E-15 5.00E-12 1.25£-12 7.69E-16 8.00E-14 2.00E-14 8.76£-16 2.00E-12 5.00E-13 1.45E-14 4.00E-12 1.00E-12 '/9/198? 12.27E-15 8.51E-16 4.OUt-U 1.WE-ll !.75E-15 1.34E-15 ~QQ{-12_ 6/1988 11.07E-15 15.00E-12 1.25E-12 1.47E-16 8.00E-14 2.00E-14 4.44E-16 2.ooE-12 5.00E-13 4.01E-14 4.ooE-12 1.00E-12 8/1988 1.98E-15 5.00E·12 1.25E-12 1.25E-15 8.00E-14 2.00E-14 6.40E-16 2.00E-12 5.00E-13 1.07E-14 4.00E-12 1.00E-1: -,----------~OOE-12 1.25E-12 3.4lE-15 8.00E-14 2.00E-14 5.08E-16 2.00E-12 5.00E-13 1.62E-14 4.00E-12 1.00E-l: 1.99E-15 1.70E-15 {14/1989 2.3lE-15 1/13/1989 4.72E- 3E-15 1.64E-15 1.48E-15 1.90E-16 3.42E- 2.77E-16 6.65E-17 1.94E-16 )E-12 1.25E-12 2.12E-15 8.00E-14 2.00E-14 1.01E-15 2.00£-12 5.00E-13 2.47£-14 4.00E-12 1.00E-1: 15.00E-12 1.25E-12 5.73E-16 8.00E-14 2.ooE-14 5.99E-16 2.ooE-12 5.ooE-13 3.23E-14 4.ooE-12 1.00E-12 5.00E-12 1.25E-12 6.32E-16 8.00E-14 2.ooE-14 5.86E-16 2.ooE-12 5.ooE-13 6.16E-15 4.ooE-12 1.00E-12 5.ooE-12 1.25E-12 2.31E-16 8.00E-14 2.00E-14 1.77E-16 2.00E-12 5.00E-13 7.65E-15 4.00E-12 1.00E-12 5.00E-12 1.25E-12 1.71E·15 8.00E-14 2.00E-14 1.52E-15 2.00E-12 5.ooE-13 1.89E-14 4.00E-12 1.00E-12 5.00E-12 1.25£-12 8.39E-16 8.00£-14 2.00E-14 8.3lE-16 2.00E-12 5.00E-13 2.57E-14 4.00E-12 1.00E-12 5.00E-12 1.25E-12 1.47E-15 8.ooE-14 2.ooE-14 1.04£-15 2.00E-12 5.ooE-13 1.79E-14 4.00E-12 1.00E-12 5.ooE-12 1.25£-12 1.49E-15 8.00E-14 2.00E-14 3.34E-16 2.00E-12 5.ooE-13 8.27E-15 4.00E-12 1.00£-12 5.00£-12 1.25£-12 7.50£-16 8.00£-14 2.00E-14 5.8OE·16 2.00E-12 5.00E-13 2.16E-14 4.00E-12 1.00E-12 15.00E-12 1.25E-12 3.48E-17 8.00E-14 2.00E-14 7.91E-17 2.00E-12 5.00E-13 3.79E-14 [4.00t- 5.00E-12 1.25E-12 1.34E-15 8.00E-14 2.00E-14 7.39E-16 2.00E-12 5.00E-13 1.46£-14 4.00~- 5.00E-12 1.25E-12 4.17E-17 8.ooE-14 2.ooE-14 1.45E-16 2.00E-12 5.00E-13 1.80£-14 . - 5.00E-12 1.25E-12 9.13E-17 8.00£-14 2.00E-14 2.77E-17 2.00E-12 5.00E-13 1.06E-14 5.00E-12 1.25E-12 4.28E-17 8.00E-14 2.00E-14 4.08E-17 2.00E-12 5.00E-13 3.51£-14 : l.>4t-10 5.ooE-12 1.25E-12 6.49E-16 8.ooE-14 2.00E-14 6.86E-17 2.ooE-12 5.00E-13 1.38£-14 OE-1 .OOE-12 4.00E-12 )E-1 l.()OE-12 1.00E-12 8/10/1992 1.73E-16 5.00E-12 1.25E-12 1.55E-16 8.00E-14 2.ooE-14 1.20E-16 2.ooE-12 5.00E-13 1.53E-14 11/9/1992 1.56E-16 5.00E-12 1.25E-12 3.19E-: 2/9/1993 2.10E-16 5.00E-12 1.25E-12 18.ooE-14 12.oo£-14"13.89E-17 .OOE-16 2.30E-16 1.82E-16 '/1994 19.18E-17 1.77E-16 2.70E-16 5.00E-12 5.00E-12 5.00E-12 9.00E-14 9.00E-14 9.00E-14 l.25E-12 4.11E-17 l.25E-12 6.00E-17 1.25E-12 L25E-12 5.00E-18 1.25E-12 2.70E-16 L25E-12 2.70E-: L.l!lt-1l13.60E-16 U5E-14 9.70E-17 U5E-14 5.36E-16 U5E-14 1.60E-16 .OOE-14 .OOE-14 .OOE-14 .OOE-14 .OOE-14 2.00E-14 2.ooE-14 2.00E-14 6.43E-17 2.00E-14 6.43E-17 2.00E-14 O.OOEtOO 2.00E-14 4.30E-17 .ooE-14 .ooE-14 :>E-1~ 5.00£-15 1.60E-15 5.00£-15 2.76E-16 2.00£-12 2.00E-12 9.ooE-13 .00£-13 :-14 .00E-13 1.60E-14 .00E-13 1.57£-14 5.00E-13 2.59E-14 OOE-13 1.60E-14 OOE-13 2.00£-15 .00E-13 2.ooE-· .25£-13 8.60E-15 t25E-13 3.84E-15 U5£-13 3.76E-15 4.00E-12 4.00E-12 4.00E-12 16.00E-1 1.00E-12 1.00£-12 1.00E-12 IDate . 'n Limit = IBHV-IU Effluent Concentration limit = Effluent Concentration limit ALARA Goal = ALARA Goal = (Pre 1994 MPC Limit = 5E-] Pre 1994 MPC limit -Pre 1994 MPC limit = ~ GOAL = 1.25t-[Pre 1994 ALARA GOAL = Cone EFC Cone EFC EFC A Cone EFC 4,80E-15 9.ooE-14 6.4lE·16 2.ooE-14 5.00E·15 8.93E-16 9.ooE-13 12/5/1996 15.34E-15 19.ooE-14 12.25E-14 [2.30E-15 12.00E.:l_' _~E-15 11.30E-15 [9.00E-13 5/6/1996 15.11E·16 19.00E-14 12.25E-1413.06E-16 12.ooE-14 [5.00E-15 11.40E·16 [9.00E-13 5.99E·16 1.55E-15 2.03 ,-16 11/6/1996 3.38E·16 9.00E-14 2.25E-14 5.45E-16 2.ooE-14 5.ooE-15 l.(Xk-l b ~;UJUt-l.:l 2/6/1997 1.00E-~6 9.ooE-14 2.25E-14 1.25E-16 2.ooE-14 5.00E-15 1.28E-16 9.00E· 5/5/1997 I1.09E-16 19.ooE-14 [2.25E-14 11.00E-16 12.ooE-14 15.00E-1511.00E·16 19,9QE-"!L 1/11/1997 2.88E-16 3.83E-16 1.82E·16 9.00E-13 lI5/1998 3.24E-16 9.00E·14 2.25E-14 3.47E-16 2.00E-14 5.00E-15 1.19E·16 9.ooE-13 4.75E-16 9.00E·14 2.25E-14 6.73E-16 2.ooE-14 5.00E-15 5.69E-16 9.00E· 8.84E-16 9.ooE·14 2.25E-14 1.93E-15 2.ooE-14 5.ooE-15 1.43E-15 9.UOt-H 2.81E-16 9.ooE-14 2.25E-14 2.89E-16 2.ooE-14 5.ooE-15 1.80E-16 9.ooE·13 12/28/1998 8.08E-16 9.ooE-14 2.25E-14 4.93E-16 2.ooE-14 5.00E-15 5.01E-16 9.ooE-13 3/29/1999 2.06E-16 9.00E-14 2.25E-14 2.06E-16 2.00E-14 5.ooE-15 1.42E-16 9.ooE- 7/3/1999 5.31E-16 9.ooE-14 2.25E-14 2.47E·16 2.00E-14 5.ooE-15 2.23E-16 9.ooE- 8.98E-16 9.00E-14 2.25E-14 3.90E-16 2.OOE-14 5.00E-15 2.96E-16 9.00E-J Effluent ALARAGoal = Pre 1994 MPC limit = f==-:_tP~"~1~'~94",ALARA GOAL = EFCA Cone 2.25E-13 5.20E-15 2.25E·13 [4.20E-15 2.25E·13 17.03E-15 l.25E·13 5.94E-15 2.25E·13 1.22E-14 2.25E·13 5.68E· 2.25£-13 14.39£-15 l.25£·13 5.29£-15 l.25E·13 4.73£-15 5.94E· 2.25E-13 5.2lt·1~ 2.25E-13 4.64E·15 t25£-13 1.06E·14 '9E-15 ,.44E- ·13 uCi/ml 14E-12 uCi/ml 1E-12 uCi/ml EFC EFC A 6.ooE·13 1.50E-13 6.ooE-13 [1.50E-13 6.00E-13 11.50E-13 6.00E-13 1.5OE-13 6.00E-13 1.5OE-13 6.00E-13 1.5OE-13 6.00E-13 11.50E-13 6.00E-13 1.50E-13 6.00E-13 1.50E-13 6.00E-13 1.50E-13 6.00E-13 1.50E·13 6.ooE-13 1.50E-13 6.00E·13 1.50E·13 OE·13 1.50E-13 .00E·13 1.50E-13 1.48E·15 9.ooE-14 2.25E-14 6.00E·16 2.00E-14 5.00E-15 5.57E-16 9.00E-13 2.25E·13 6.19E-15 6.00E·l 1.50E-13 1.5OE-13 1.00E-16 9.00E-14 2.25E-14 1.06E·16 2.00E-14 5.00E-15 l .ooE-16 9.00E·13 2.25E-13 6.23E-15 6.00E-13 1.50E-13 16/26/2000 3.47E-16 9.ooE-14 2.25E·14 3.46E-16 2.OOE-14 5.00E-15 3.62E-16 9.00E-13 2.25E·13 4.50E-15 6.00E-13 1.50E-13 9/26/2000 2.51E-16 9.00E-14 2.25E·14 1.78E-16 2.00E-14 5.00E-15 3.25E-16 9.00E-13 2.25E·13 8.55E-15 6.ooE-13 1.50E-13 --.--.----l.ooE-16 9.ooE-14 2.25E-14 1.42E-16 2.ooE-14 5.ooE-15 1.3lE-16 9.ooE-13 2.25E-13 7.77E-15 6.00E-13 1.50E-13 ------------------i.OOE-13 1.50E-13 /2002 3.55E-16 4.85E-16 1.06E-16 7.65E-15 6.00E-13 1.50£-13 .17E-16 1.61E-16 1.00E-16 3.68E-15 1.50E-13 12/30/2002 3/31/2003 6/30/2003 .OOE-16 19.ooE-14 12.25E-14 1.03E-16 2.00E-14 5.ooE-15 1.00E-1- 1.12E-16 2.00E-14 5.00E-15 1.00E-1- 18E·16 19.00E-14 1 2.25E-14 3.40E-16 2.OOE-14 5.ooE-15 1.67E-l OOE·16 9.00E-14 2.25E-14 1.00E-16 2.ooE-14 5.ooE-15 1.00E-1 l.OOE-16 19.ooE-14 12.25E-14 2.54E-16 2.ooE-14 5.00E-15 13.35E-16 6/27/200 9/27/200 12/27/20 l.ooE-16 ...J:9.ooE-14 2.25E-14 1.00E-16 2.00E-14 5.ooE-l~-+I.00E-16 -14 -+2.25E-14 1.ooE-16 2.ooE-14 5.00E-15 ~ 1.00E-16 3/2006 2.13E-16 3/2006 1.62E-16 7/3/2006 1.86E-16 [10/2/2006 11,ooE-16 [1/1/2007 11.00E·16 4/2/2007 7/2/2007 9/30/2007 -_. __ ._--- 1.14E-16 7.09E-16 7.69E-16 1.24E·15 E-14 9.00E-14 IE-14 )OE-14 I.00E-14 9.00E-14 E-14 E-14 l.ooE-14 I.OOE-14 9.00E·14 E·14 E-14 19.00E-14 E-14 1.00E-16 2.00E-14 5.00E-15 -------------------- E-14 2.25E-14 1.30E-16 2.25E-14 2.56 2.25E-14 1.04 2.25E-14 1. 2.25E-14 [1.ooE-: 2.25E-1411.00E-16 2.25E-14 [1.47E-16 .25E-14 .25E- .25E- 25E-14 2.25E-14 1.13E-16 2.25E-14 3.83E-16 2.25E-14 2.94E-16 :-14 :-14 :-14 2.25E-14 19.25E-17 E-14 ~.OOE-14 OOE-14 .OOE·14 .ooE-14 ooE-14 12,OOE-14 12.00E-14 E-14 E-14 E-14 E-14 :-14 :-14 OE-l' 1.20E-16 2.42E-1I ... :, e·OOE~l~ 1.00E- 5.ooE-15 11.ooE-1 5.00E-15 11.00E-16 5.00E-1511.00E-16 '-1 '-1 ;.OOE-15 1.00E-16 "OOE-15 2.27E-16 5.ooE-15 1.90E-16 1.34E-16 l.OOE-15 ~.18E J.87E- 12.ooE-14 [5.ooE-15 15.60E-17 9.00E-13 9.00E-13 9.00E-13 9.00E-13 9.ooE-13 9.00E-13 9.00E-13 9.00E-13 1.00E-13 1.00E-13 1.00E-13 9.ooE-13 2.25E-13 6,25E-15 2.25E-13 1.54E-14 2.25E-13 7.94E-15 2.25E-13 1.22E-14 2.25E-13 13:73E-14 2.25E- 1.25E-13 19.77E-15 2.2~~·13 11.30E-14 2.25E·13 11.17E-14 -14 E-14 5.44E-15 2.25E-13 6.52E-15 2.25E-13 7.54E-15 1,25E-13 [1.16E-14 16.ooE-13 6.ooE-13 6.00E-13 6.00E-13 16.00E-13 1 600'-16.ooE-13 16.ooE~13 [6.ooE-13 6.00E-13 6.ooE-13 16.ooE-13 1.50E-13 1.50E-13 1.50E-13 1.50E-13 1.50E-13 1.50E-13 1.50E-13 1.50E-13 1.50E-13 1.50E-13 l~OE-13 1.50E-13 1.50E-l 1.50E-13 1.50E·13 -13 ,-13 ,-13 ,-13 Dilte Effluent Concentration Limit = 9E-14 uCi/ml BHV-1U Effluent Concentration limit = 2E-14 uCi/ml BHV-lT Effluent Concentriltion limit = 9E-13 uCi/ml BHV-1R Effluent Concentration limit = 6E-13 uCi/ml BHV-1PB ALARAGoal = 2.25E-14 uCi/ml ALARAGoal = 5E-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml Pre 1994 MPC limit :: SE-UuCi/ml Pre 1994 MPC limit: 8E-14 uCi/ml Pre 1994 MPC Limit -U -UuCi/ml Pre 1994 MPC limit = 4E·UuCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA 3/31/2010 1.97E-15 9.ooE-14 2.25E-14 2.15E-16 2JXIE-14 5.ooE-15 3.27E-16 9.ooE-13 2.25E-13 1.ooE-14 6.ooE-13 1.50E-13 6/30/2010 1.58E-15 9.ooE-14 2.25E-14 4.71E-16 2.ooE-14 5.ooE-15 7.70E-16 9.ooE-13 2.25E-13 4.07E-15 6.00E-13 1.50E-13 9/30/2010 8.42E-16 9.ooE-14 2.25E-14 2.8OE-16 2.ooE-14 5.00£-15 1.31E-16 9.ooE-13 2.25E-13 6.8OE-15 6.00£-13 1.50£-13 12/31/2010 1.27E-15 9.00£-14 2.25E-14 2.32E-16 2.ooE-14 5.00£·15 2.30E-16 9.ooE-13 2.25E·13 1.27E-14 6.00E-13 1.50E-13 VI C o ~ -c CII u c o () CII :5! (j :::l c .2 "C ~ .... ::> J: EO N ~ , w 0 C> ~ (") ~ , w 0 C> ~ • +:: I~ :::::. r-. ,~ .. .:: ~ 4<: ~ ,,- ~ --.. 4( -' ~ ~ t. ... -;t ::t -.. --' 1 ~ ... ~ , w 0 C> ~ r---.. .... I , ~ I ... I~ I ~ ~ , ,,. , I ~,. I ~~ ~ '" ~ , w 0 C> (aIB:JS 501) 60-das -\lo-das ~ -I·r-. ~ ~ ~ ,. Lo-das 90-das 90-das , vo-das .: ~ £o-das lO-daS 0 ~ N -. ........, , ~o-das "0 ro .3 "!Jf! ... OO-daS + 66-daS to N \l6-das N , E :7 :::;Il L6-das ::J 'i5 ro c:: ;......-' '"'" .. - 96-das + 96-das 0 v6-das (") N , E • ~ ? I - ~ - £6-daS ::J 'C 0 .I:: l6-daS f- + ~6-das -06-daS "iii .a 6\l-das ro z E \l\l-das ::J '1: ro L\l-daS ~ ::J 9\l-daS + ... 9\l-das v\l-das -£\l-daS l\l-das ~\l-das to "-00 ~ ~ ~ , , , w w w 0 0 0 C> C> C> ~ ~ ~ 1.00E-11 1.00E-12 1.00E-13 Q) ro " (l)1 .00E-14 OJ o do 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml -, J. .}.~ .H 1 \. • 1\ ¥" ¥ r-V -. I ~ • V ~ N "" .... I{) <0 I"-co OJ a co co co co co co co co co '" , , 6. 6. 6. 6. 6. 6. 6. 6. 0. 0. Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol (I) (I) (I) (I) (I) (I) (I) (I) (I) (I) ~ ., iT'" • ~ N "" '" OJ OJ 6. 6. 6. Ol Ol Ol (I) (I) (I) BHV-1 Uranium-Natural Concentrations (uCi/ml) ... ~ 1\ /"\J - JI. I~ 1\ 1 ... . \!v J. \/ j J~j ... - .... I{) <0 I"-co OJ a ~ N "" .... I{) <0 I"-co '" a OJ OJ OJ '" '" '" a a a a a a a a a a ~ 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. , , , , 0. 0. 0. 0. Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol (I) (I) (I) (I) (I) (I) (I) (I) (I) (I) (I) (I) (I) (I) (I) (I) (I) E -U :::J -III I: o :;; ~ .. I: Q) (J I: o U o M N , E :::J ';: o .s:: .... ..... ::> J: III I N C') ~ ~ uJ , W a a C> a ~ ~ t:: I ....... " .. ~"---'<t LO ~ ~ , , W W a a C> C> ~ (aI8:)8 BOl) ~ -40 [.-" I 60-daS 9O-daS K I., ~ LO-daS 90-daS 9O-daS vO-daS I" £o-das ~ lO-daS ... r---. .-' ~o-das b-f7 OO-daS ~ 66-daS g6-das L6-das ~ 96-das g6-das ~ v6-das £6-das l6-das I ~6-das , 06-daS 6g-das gg-das L9-daS 99-daS -. gg-daS vg-das -. £g-das I 19-das ~g-das CD ,.... co ~ ~ ~ , , , W W W a a a C> C> C> ~ ~ ~ 1.00E-11 1.00E-12 1.00E-13 _1.00E-14 '" ~ CfJ Cl o -' ~1.00E-15 1.00E-16 1.00E-17 1.00E-18 Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml rr/\ ~ ~ ~ • ~ N (') ... L{) co r-. <Xl '" a <Xl <Xl <Xl <Xl <Xl <Xl <Xl <Xl <Xl '" , 6. 6. 6. 6. 6. 6. 6. 6. , a. a. '" '" '" '" '" '" '" '" '" '" CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ \ T i I ~ 1 ~ N (') ... '" '" '" '" , , , , a. a. a. a. '" '" '" '" CfJ CfJ CfJ CfJ BHV-1 Radium-226 Concentrations (uCi/ml) ~ 1 .. \ • 1\ • .1 JI~ ¥ ~ J\.. J.J. \ .J\ Ai \ ~ L{) co r-. <Xl '" a ~ N (') ... L{) co r-. <Xl '" a '" '" '" '" '" a a a a a a a a a a ~ , , , , , , , , , , , , , , , , a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. '" '" '" '" '" '" '" '" '" '" '" '" '" '" '" '" CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ 1.00E-11 1.00E-12 1.00E-13 Q) ro u en1 .00E-14 Cl o --' 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994ALARA Goal = 1E-12 uCilml ..JI ~.J /\/\ I/~ ,1 A 1. ~ ~ V T \, ~ N cry ... '" CD .... 00 '" 0 00 00 00 00 00 00 00 00 00 '" , , , , , , , , , , a. a. a. a. a. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) en en en en en en en en en en , It ¥)J VV+ ~ N cry '" '" '" , , , a. a. a. Q) Q) Q) en en en BHV-1 Lead-210 Concentrations (uCi/ml) II t ... J.. J ~ \~ . 1 ... '" CD .... 00 '" 0 ~ N cry ... '" CD .... 00 '" 0 '" '" '" '" '" '" 0 0 0 0 0 0 0 0 0 0 ~ , , , , , , , , , , , , , , , a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) en en en en en en en en en en en en en en en en en TAB 2 BHV-2 AIR SAMPLING GRAPHS AND DATA TABLE IDate IEffluent ' .. = 19E-14 uCi/ml IBHV-2u IEffluent Concentration limit = 12E·14 uCi/mIIBHV-2T IEffluent Concentration limit = 19E-13 uCi/ml IBHV-2R IEffluent Concentration limit = 16E-13 uCi/ml IBHV-2PB II = 2.25E-14 uCi/ml ALARAGoal = 5E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC limit = 5E-12 uCi/ml Pre 1994 MPC limit = 8E-14 uCi/ml Pre 1994 MPC limit = 2E-12 uCi/ml Pre 1994 MPC limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFC A Cone EFC EFC A Cone EFC EFC A Cone EFC EFC A 1.39E-15 5.ooE·12 1.25E-12 3.69E-16 8.ooE·14 2.ooE-14 5.92E-16 2.ooE·12 5.ooE-13 1.67E·14 4.ooE·12 l.ooE-12 l/14/1981 4.62E-16 5.ooE·12 1.25E-12 8.03E-16 8.ooE·14 2.ooE-14 3.62E-16 2.ooE·12 5.ooE-13 1.33E-14 4.ooE-12 1.ooE·12 '0-/1982 7.07E·16 5.ooE·12 1.25E-12 1.10E·15 8.ooE·14 2.00E-14 7.27E-16 2.ooE·12 5.ooE-13 1.52E·14 4.ooE-12 1.ooE-12 1/1982 8.84E-16 5.00E·12 1.25E-12 7.73E-16 8.00E-14 2.ooE-14 4.78E-16 2.00E·12 5.00E·13 1.98E·14 4.ooE·12 1.00E·12 /1982 1.23E-15 5.00E·12 1.25E-12 3.60E·16 8.00E-14 2.00E-14 8.73E-16 2.00E·12 5.00E-13 2.35E·14 4.ooE·12 1.00E·l;' 183 12.64E-15 15.00E·12 Jl}~E.1212.55E·16 18.00E·14 12.00E·1411.98E-16 12.00E·12 15.00E-1312.85E·14 14.ooE-12 11.00E-12 1/1983 2.14E-16 5.00E-12 1.25E-12 1.02E-16 8.00E-14 2.00E·14 1.57E-16 2.00E·12 5.00E·13 2.48E-14 4.00E·12 11.00E-12 0/1983 2.85E-16 5.00E·12 1.25E·12 2.06E·16 8.00E-14 2.00E·14 2.24E-16 2.00E·12 5.00E-13 1.79E·14 4.00E·12 1.00E·12 3/1983 2.70E-16 5.00E-12 1.25E-12 3.36E-16 8.00E·14 2.00E-14 4.37E-16 2.ooE·12 5.00E-13 1.78E·14 4.00E-12 1.00E·12 /1984 2.78E·15 5.ooE-12 1.25E-12 1.20E·16 8.ooE·14 2.ooE·14 6.64E-17 2.ooE-12 5.ooE-13 9.14E-15 4.00E-12 L.OOE·l; ·1984 4.28E·16 5.ooE-12 1.25E-12 1.75E·16 8.00E·14 ?OOE·14 4.57E·17 2.ooE-12 5.ooE-13 3.55E-14 4.ooE·12 l.()QE-12 ~ Z.78E·15 8.12E·16 1.98E-16 1.68E-14 14.ooE-l l.ooE-12 1.ooE-12 110/1/1984 1/2/1985 ~/1/1985 7/1/1985 2.69E·16 2.66E-17 8.ooE-14 2.00E·14 O.OOE-+OO 2.ooE-12 5.00E-13 1.77E- 2.15E·16 7.55E-16 8.ooE-14 2.ooE·14 2.87E-16 2.00E-12 5.ooE·13 3.19E·14 4.ooE·12 l.UOI::-12 1/2/1986 4/1/1986 6/30/198E 15/11/1987 /1987 2/1981 DOE·17 9.32E·17 1.00E- .31E· .23E· S.4lE-l 3.56E·16 5.3lE-16 4.06E-16 .74E·16 .73E-16 .78E-15 63E·16 8.06E·16 11/14/1988 4.34E-16 2/13/1989 5.8OE-16 5/15/1989 5.06E-16 5/14/1990 8/13/1990 ., "",QQ('J /11/1991 10/1992 U IE·16 1.14E·15 8.72E-li 1.16E·16 L.OIE·16 5.20E-17 '2/9/1993 -)2.39E·16 5/10/1993 1.00E·16 8/10/1993 1.90E· 11/8/1993 1.00E-16 !/7/1994 2.23E·16 15/9/1994 2.16E-16 18/9/1994 19.29E-17 E-17 1.18E· 9.40E- 8/9/1995 8.90E-17 IS.ooE-ll l .l!lt-ll 1.b7E-lb 8.ooE-14 1.00E·14 6.75E·17 2.00E-12 5.00E·13 7.56E-15 14.ooE·12 15.00E·12 1.25E-12 9.00E·16 8.00E-14 2.00E·14 4.90E-17 2.ooE-12 5.ooE-13 1.31E-14 4.00E·l #.OOE-12 1.25E-12 2.18E·16 8.00E-14 2.00E·14 3.71E·16 2.00E-12 5.00E·13 3.64E-15 '+4.00E-1 :!Q!:-12 1.25E-12 2.16E-16 8.00E·14 2.ooE·14 2.15E-17 2.00E-12 5.00E·13 3.04E- 1.50E-16 8.00E-14 2.00E-14 3.71E·16 2.00E-12 5.00E·13 2.90E-15 14.00E-12 ·12 11.25E-12 1.32E·16 8.00E-14 2.00E-14 7.09E·17 2.ooE-12 5.ooE·13 2.53E-14 .14.00E-12 ~ ~ ~ ~ ~ 1.00E-12 £.ooE-12 1.25E-12 1.74E·16 8.ooE·14 2.ooE-14 3.67E·16 2.ooE-12 5.ooE·13 I.04E-14 14.ooE·l 15.ooE·12 1.25E-12 l.ooE-16 8.ooE-14 2.ooE-14 1.05E·16 2.ooE-12 5.ooE·13 7.81E·15 1.00E·12 ¥.ooE-12 1.25E-12 1.30E·16 8.00E·14 2.ooE-14 7.74E·17 2.ooE-12 5.ooE·13 3.80E-14 ~E-12 1.25E·12 6.63E-17 8.00E-14 2.ooE-14 1.34E·16 2.ooE-12 5.ooE·13 1.10E-14 4.1)I)1:.-1.L 1.1)I)1:.-ll I 2.38E-16 8.ooE-14 2.ooE-14 1.38E·16 2.ooE-12 5.ooE·13 I.04E-14 4.ooE-12 l.ooE-IU ·12 11.25E.12 3.11E-16 8.ooE-14 2.ooE-14 1.83E-16 2.ooE-12 5.00E·13 1.17E-14 4.00E-12 1.ooE-IU 5.ooE-12 1.25E·12 2.3IE-17 8.00E·~!.... 2.ooE-14 1.20E-16 2.00E-12 5.00E·13 3.55E-14 4.ooE-12 1.ooE-12J 5.00E-12 1.25E-12 1.49E-16 8.00E-14 2.00E-14 2.30E-16 2.00E-12 5.00E·13 1.18E-14 4.00E-12 1.00E-12- 5.00E-12 1.25E-12 8.69E-16 8.ooE-14 2.00E·14 1.8OE·16 2.00E-12 5.00E-13 1.42E-14 4.00E·12 1.00E·l~ 5.00E·12 1.25E-12 6.76E-16 8.00E-14 2.00E-14 1.57E-16 2.00E-12 5.00E-13 2.25E-14 4.00E-12 1.00E-12 ·12 1.25E·12 2.85E·16 8.00E-14 2.ooE-14 1.55E-16 2.00E-12 5.00E·13 2.80E-14 4.00E-12 l.ooE-12 5.00E-12 1.25E-12 2.28E-16 8.ooE·14 2.00E-14 1.63E-16 2.00E-12 5.ooE·13 6.05E·15 4.ooE-12 1.ooE-12 5.ooE-12 1.25E-12 9.60E-16 8.00E·14 2.ooE-14 1.26E-15 2.ooE-12 5.ooE-13 6.65E-15 4.ooE-12 1.00E-12 5.00E·12 1.25E-12 4.08E-16 8.ooE-14 2.ooE-14 4.18E-16 2.ooE-12 5.ooE-13 1.59E-14 4.ooE·12 1.00E·12 IE·12 1.25E·12 3.25E·16 8.00E-14 2.00E-14 3.74E-16 2.00E·12 5.00E·13 1.98E-14 4.ooE-12 1.00E-12 5.27E-16 8.00E·14 2.00E-14 3.97E-16 2.00E-12 5.00E·13 1.69E·14 4.ooE-12 1.00E-12 ·12 1 1.25E-1215.49E-16 8.00E-14 2.00E-14 4.75E-17 2.00E-12 5.ooE-13 1.27E-15 4.00E·12 1.00E-12 .00E·12 11.25E-1212.64E-16 18.00E-14 12.ooE-14 1.93E-16 2.00E-12 5.00E-13 2.25E-14 4.ooE-12 1.ooE-12 5.00E-12 -+1.25E-l~-lrOOE-18 8.00E·14 12.ooE-14 3.33E-17 2.00E-12 5.00E-13 3.49E-14 4.ooE-12 l .ooE-12 8.00E·14 -+.2.00E-14 2.80E-16 2.00E-12 5.ooE-13 1.50E-14 4.ooE-12 1.ooE·12 5.ooE·12 5.ooE-12 5.00E·12 IE-12 ooE-12 5.00E-12 5.00E-12 .ooQ4 1.25E-12 7.63E·17 1.25E-12 7.07E·17 1.25E-12 3.65E-17 1.25E-12 2.97E-17 ;·16 1.25E-12 1.00E·16 1.25E-12 l.ooE-16 1.25E·12 7.20E·17 E·14 2.25E-1419.67E·17 7.65E-17 2.00E-12 5.ooE-13 1.58E-14 4.ooE-12 1.00E·12 8.00E·14 2.00E-14 2.54E-17 2.00E-12 5.ooE·13 1.45E·14 4.ooE-12 1.ooE-12 8.ooE·14 2.00E·14 1.4OE-17 2.ooE-12 5.ooE-13 3.4lE-14 4.ooE·12 l .ooE·12 8.ooE-14 2.00E-14 3.07E-17 2.ooE·12 5.ooE-13 1.27E-14 8.ooE·14 2.00E-14 2.80E-17 2.(MlE-12 5.ooE-13 1.41E-14 :!Q!:-14 2.00E-14 1.78E-17 2.ooE-12 5.00E- .OOE-14 6.31E-17 2.00E-12 5.00E-lili.41E-14 E-14 LOOE-14 8.00E-14 8.00E-14 E·14 OE-] . .JQl-14 3.19E-17 2.00E-12 5.ooE-1311.34E-14 LOOE,I; OOE-14 1.00E-16 2.00E-12 5.00E·1311.8OE-14 ~ 4.00E-12 2.00E-14 1.00E-16 2.00E-12 5.00E-IW..49E-14 2.00E·14 1.84E·16 2.00E-12 5.00E-l 9.89E-17 2.ooE-12 5.ooE·13 11 . .;Sfl:.-14 4.WI:.-ll 11.wl:.·l.! • -'E·16 2.ooE-12 5.00E-13 1.00E-16 4.00E-12 1.ooE-12 E-16 2.00E-12 5.00E·13 11.00E-16 4.00E-12 11.00E-12 .. ~ ---~.. ..~~ .. ~-.~.~ <;-.... .3 1 , ...... <;-.1.3 16.ooE-13 11.50E-13 E-14 3.5OE-1 9.ooE-13 9.00E-13 2.25E·13 3.90E-15 1.50E·13 !.OOE·14 1.35E-16 2.25E-13 2.38E-16 1.50E-13 1 Date 11/11/1995 2/5/1996 5/6/1996 1~/5/199.§_ /1997 /1997 1/1997 /1998 1/28/1998 ,2/28/1998 IEffluent· n Umit= 19E-14 uCl/ml IsHV-zu I limit = IZE-14 uCl/mll BHV-ZT Effluent Concent~tion limit = 9E-13 uCl/ml ISHV-2R IAU Pre 1994 MPC limit = Ipre 1994ALARA GOAL = Cone 2.83E·15 1.75E· 1.40E·16 1.43E·16 1.45E-16 1.00E-16 ALARA Goal = 2.2 ..... -1.5E-13 uCl/ml .I..,Ut;-,U u .... 'ml Pre 1994ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL = .OOE- '.OOE- IOE-14 EfC A Cone EfC EfC A Cone EfC EfC A Cone EfC EfC A 1 2.25E-14 4.09E·16 2.00E-14 5.00E·15 5.23E-16 9.00E-13 2.25E-13 6.77E-15 6.OOE·13 1.50E-13 2.25E-14 8.66E·16 2.00E-14 5.00E-15 4.86E-16 9.00E-13 2.25E·13 3.50E·15 6.00£-13 1.50£-13 1 .. "~r •••. 15E.16 2.00E-14 5.00E·15 1.00E·16 9.ooE-1~ 2.25~13. 6.85E-15 6.OOE·13 1.50E-13 1 9.00£-14 2.25E-14 2.78£·16 2.ooE-14 5.00E·15 1.00E·16 9.00E-13 2.25E·13 5.83E-15 6.00E-13 1.50E-13 9.ooE-14 2.25E-14 1.57E-16 2.ooE-14 5.00E·15 1.00E-16 9.ooE-13 2.25E·13 1.19E-14 6.OOE-13 1.5OE-13 1 9.ooE-14 2.25E-14 1.ooE-16 2.ooE-14 5.00E-15 1.00f·16 9.ooE-13 2.25E·13 5.84E-16 6.OOE-13 1.50E-13 9.ooE-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00f-16 9.ooE-13 2.25E·13 3.89E-15 6.OOE-13 1.5OE-13 1 l.UOt-lb 19.UOE-14 ILl!)t·1411.09E-lb 12.ooE-14 15.00E-1511.00E·16 19.ooE-13 12.25E-13 15.69E-15 16.00E-13 11.50E-13 2.55E-16 19.00E-14 12.25E·14 h .07E-16 12.ooE-14 15.00E-1515.00E·17 19.ooE-13 12.25E-13 15.11E-15 6.OOE-13 1.50E-13 1.20E-16 -!?OOE-14 +.2.25E-1W .71E-16 +.z.OOE-14 ~.OOE-l~+'1.28E'16 -!?ooE-13 +.2.25E.13 16.40E-15 6.00E-13 1.50E-13 4.80E-15 6.OOE-13 1.50E-13 6.OOE-13 1.50E-13 1.47E-16 9.00E·14 2.25E·14 4.24E-16 2.00E-14 5.00E-15 3.39E-16 9.00E-13 1.00E-16 9.00E·14 2.25E·14 1.00E-16 2.ooE·14 5.00E-15 1.00E-16 9.ooE-13 12.25E.I314.26E-15 2.54E-16 9.00E·14 2.25E·14 2.15E-16 2.ooE·14 5.00E-15 1.38E·16 9.00E-13 2.25E·13 16.88E-15 6.00E-13 -t,.50E-13 l.o?E-16 9.00E·14 2.25E·14 1.00E-16 2.ooE-14 5.00E-15 1.00E-16 9.ooE·13 .12.25E-l!lZ.61E-15 .16.ooE-13 ..l!.50E-13 ,,3/1999 2.46E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.95E-15 6.OOE-13 1.50E·13 9/27/1999 2.81E-16 9.00E-14 2.25E-14 1.41E-16 2.ooE-14 5.ooE-15 1.00E-16 9.00E-13 2.25E-13 7.35E·15 6.ooE-13 1.50E-13 12/28/1999 5.20E-16 9.00E-14 2.25E-14 2.60E-16 2.ooE-14 5.ooE-15 2.01E-16 9.00E-13 2.25E-13 7.00E-15 6.OOE-13 1.50E-13 3/27/2000 1.00E-16 9.00E·14 2.25E-14 1.00E-16 2.00E·14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.12E-15 6.OOE-13 1.50E-13 L/2002 17/1/2002 1.10E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.ooE-15 1.16E-16 9.00E-13 2.25E-13 5.07E-15 6.ooE-13 1.50E-13 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E·14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 5.31E-15 6.ooE-13 1 "M_1:t I()E-1 l.OOE-16 ,. nn ... ., 1.50E-13 OOE-14 2.25E-14 1.00E-16 2.00E-14 5.00E·15 1.00E-16 9.00E-13 2.25E-13 6.16E-15 6.OOE-13 1.50E-13 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 2.20E-15 6.00E-13 1.50E-13 OOE-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 9.95E-15 6.00E-13 1.5OE-13 .OOE-14 2.25E-14 1.43E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 8.25E-15 6.00E-13 1.5OE-13 .OOE-16 19.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E·16 9.00E-13 2.25E-13 3.69E-15 6.OOE-13 1.5OE-13 :)E-16 9.00E-14 _ 2:~?E~.!4 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.91E-15 6.OOE-13 1.50E-13 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E·13 6.16E-15 6.OOE-13 1.50E-13 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 5.27E-15 6.00E-13 1.50E-13 /2003 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.23E-15 6.00E-13 1.50E-13 9/2003 1.00E-16 9.ooE-14 2.25E-14 1.00E-16 2.ooE-14 5.00E-15 1.00E-16 9.ooE-13 2.25E-13 7.80E-15 6.OOE-13 1.50E-13 ._---l!:.ooE-16 9.ooE-14 2.25E-14 1.00E-16 2.ooE-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 2.04E-14 6.OOE-13 1.50E-13 DE-16 9.ooE-14 2.25E-14 1.00E-16 2.00E·14 5.00E-15 1.00E-16 9.ooE-13 2.25E-13 3.09E-15 6.OOE-13 1.50E-13 11.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E·13 2.25E-13 1.73E-14 ;j2006 h :29E-16 19.00E-14 12,25E.:.14J~,90~:I~ 12.ooE-14 15.00E-15 14.08E-16 19.ooE-13 12.25E-1316.58E-14 16.ooE-13 1.50E-13 1.50E-13 ;j2006 11.02E-16 19.00E-14 12.25E-141 1.ooE-16 12.ooE-14 15.00E-15 11.00E-16 19.ooE-13 12.25E-1311.08E-14 16.ooE-13 ;/2006 11.ooE-16 9.00E-14 2.25E-14 1.00E·16 6.00E-n 1.:;'Ut-l,;!! 1.30E-16 9.00E-14 2.25E-14 1.00E·16 2.00E-14 5.ooE-15 1.00E-16 9.00E-13 1.68E-14 6.ooE-13 1.50E-13 1.24E-16 9.00E-14 2.25E-14 1.00E-16 2.ooE-14 5.ooE·15 1.00E-16 9.ooE-13 2.25E-13 1.38E-14 6.OOE-13 1.5OE-1" /2/2007 1.40E-16 I.UUt-1Q IL.Dt-1Q Il.UUt-16 12.00E-14 15.00E-15.11.OOE-16 19.00E-13 12.25E·1311.63E-14 16.00E-13 11.5OE-13 '/2/2007 1.04E-16 1.00E-16 1.36E-14 1.5OE-13 1.00E-16 1.00E-16 8.24E-15 1.5OE-13 1.91E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.ooE-16 9.00E-13 2.25E-13 1.18E-14 6.00E-13 1.5OE-13 0/2008 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.49E-15 6.00E-13 1.50E-13 0/2008 1.29E-16 9.ooE-14 2.25E-14 1.00E-16 2.ooE-14 5.00E-15 1.00E-16 9.00E-13 2.25E·13 4.82E-15 6.00E-13 1.50E-13 0/2008 9.00E·14 2.25E-14 2.ooE-14 5.00E-15 9.ooE-13 2.25E-13 6.ooE-13 1.50E-13 _ .. ----9.00E-14 2.25E-14 2.00E-14 5.ooE-15 9.ooE-13 2.25E-13 6.OOE-13 1.50E·13 13.96E-16 1.24E-17 2.43E-16 .72E-16 ~}.OOE'14 2.25E-14 1.38E-16 2.00E·14 5.00E-15 1.07E-16 9.00E-13 2.25E-13 4.81E-15 6.ooE-13 1.50E-13 19.00E-14 2.25E-14 4.64E-17 2.00E-14 5.00E-15 5.11E-17 9.00E-13 2.25E-13 4.58E-15 6.OOE-13 1.50E-13 19.00E-14 2.25E-14 5.28E-17 2.00E-14 5.00E-15 4.84E-17 9.00E-13 2.25E-13 1.19E-14 6.ooE-13 1.50E-13 ~.OOE-14 2.25E-14 2.94E-17 2.00E-14 5.00E-15 2.57E-17 9.00E-13 2.25E-13 6.70E-15 6.OOE-13 1.5OE-13 Date Effluent Concentration limit = 9E·14 uCi/ml BHV-2U Effluent Concentration Limit = 2E-14 uCi/ml BHV-2T Effluent Concentration limit = 9E-13 uCi/ml BHV-2R Effluent Concentration Limit = 6E-13 uCi/ml 8HV-2P8 ALARAGoal = 2_25E-14 uCi/ml ALARAGoal = 5E-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARAGoal = 1.5E·13 uCi/ml Pre 1994 MPC Limit-5E-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC limit = 4E-UuCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL = 1E.UuCi/ml Cone EFC EFCA Cone £Fe EFCA Cone £Fe EFCA Cone EFC EFCA 3/31/2010 5.47E-16 9.ooE-14 2.25E-14 1.42E-17 2.ooE-14 5.ooE-15 4.66E-17 9.ooE-13 2.25E·13 8.24E-15 6.ooE-13 1.50E-13 6/30/2010 3.58E-16 9.ooE-14 2.25E-14 6.64E-17 2.ooE-14 5.ooE-15 9.90E-17 9.ooE-13 2.25E-13 2.0lE-15 6.ooE-13 1.50E-13 9/30/2010 2.91E-16 9.ooE-14 2.25E-14 4.48E-17 2.ooE-14 5.ooE-15 5.72E-17 9.ooE-13 2.25E-13 1.08E-15 6.ooE·13 1.50E·13 12/31/2010 5.73E-16 9.ooE-14 2.25E-14 7.24E-17 2.ooE-14 5.ooE-15 6.76E-17 9.00E-13 2.25E-13 1.35E-14 6.ooE-13 1.50E-13 VI c: o ~ c: Q) u c: o () Q) :2 u :l c: . 2 "0 "' 0:: N :> :J: III 1 N ~ , w 0 0 ~ • ."-. .. ... ""- \ C') ~ , w 0 C> • Ii ~ .. • ? ~ 1 ~ ~ ~ ...-A ... ~ r ~ ..,. ~ , w 0 C> ~ ~ o ~-das I ~ 60-daS K ~ so-das LO-daS 90-daS ~ SO-daS vo-das £o-das 0 ~ ~ lO-daS N , "0 >4 '" ~o-das Q) -' j oo-das + ~ ~ 66-das '"" N N S6-das , E ::J ., L6-das '0 '" 0:: to:: :4f' 96-das + ~ ~ S6-daS 0 C') v6-daS N , E ::J £6-daS ·c 0 .. 0::-"' C .. .... I:::. .<:: l6-daS f- + ~6-das J. ~ ]. 06-das 1'i .3 '" 6S-daS z E ss-das ::J 'c '" ~ • ~ ~ LS-daS ~ + 9S-daS ss-das vs-daS ...... ~ --.. ..-1 • t I £s-das lS-daS ~s-das It) '"" .... <X> ~ ~ ~ ~ , w , , w w w 0 0 0 0 C> C> C> C> ~ ~ ~ ~ (ale~s 601) III C o ~ -C GI U C o u I N C') ~ ~ , , W W a a ~ ~ ~ ~ I I ~ I --.. I <t on ~ ~ , , W W a a ~ ~ (ale:JS 601) ~ o~-das 60-daS ., ~I so-das LO-daS 90-daS 4( 9O-daS PO-daS , £o-das 4( lo-das I ~o-das ~I OO-daS ~p l I«~I , 66-daS S6-daS L6-daS ( 96-das g6-das 4( P6-das ~ ';<;:1 £6-das I· ...... I l6-das ~6-das .. 06-daS 6S-daS ss-das • Ls-das 9S-daS IJ.-A ' gs-das Ps-das ~ £s-das ls-das ~s-das <!) I'-- ~ ~ , , W W a a ~ ~ ~ ~ 1.00E-11 1.00E-12 1.00E-13 _1.00E-14 '" ro " (f) Ol o -' ~1.00E-15 1.00E-16 1.00E-17 1.00E-18 ~ <Xl 6. '" (f) Effluent Concentration Limit = 2E-14 uCilml ALARA Goal = 5E-13 uCilml Pre 1994 MPC Limit = 8E-14uCilml .. ~ .I .' '\j V 'I ~ N '" ... '" CD "-<Xl '" 0 <Xl <Xl <Xl <Xl <Xl <Xl <Xl <Xl '" 6. 6. 6. 6. 6. 6. 6. 6. 6. '" '" '" '" '" '" '" '" '" (f) (f) (f) (f) (f) (f) (f) (f) (f) ~ N '" '" '" '" 6. , 6. a. '" '" '" (f) (f) (f) BHV-2 Thorium-230 Concentrations (uCi/ml) --------------_ ... _ ... _----_ .... _- , r. I .. l! \. \ .. 1 v\j ~ .A J\ ~ --' ¥ ... '" CD "-<Xl '" 0 ~ N '" ... '" CD "-<Xl '" 0 '" '" '" '" '" 9 0 0 0 0 0 0 0 0 0 0 ~ , , , , , 6. 6. 6. 6. 6. 6. 6. 6. , , , a. a. a. a. a. a. a. a. a. '" '" '" '" '" '" '" '" '" '" '" '" '" '" '" '" '" (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) 1.00E-11 1.00E-12 1.00E-13 Q) Oi " en1 .00E-14 Ol o 2. 1.00E-15 1.00E-1 6 1.00E-17 co c. Q) en Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCilml Pre 1994 MPC limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml J N co ~ , a. Q) en '" co , a. Q) en ... co , a. Q) en .... .tiV~ "' co .... at '9 '9 a. a. a. Q) Q) Q) en en en co "i' a. Q) en '" "i' a. Q) en I J/\ ~ /\1 ~ . o ~ q> q> a. a. Q) Q) en en N ~ a. Q) en \ II IV '" ~ a. Q) en ~ a. Q) en BHV-2 Radium-226 Concentrations (uCi/ml) "' ~ a. Q) en co ~ a. Q) en .... ~ a. Q) en IA .J\... co ~ a. Q) en '" '" c. Q) en o ~ N o 0 0 6. 6. 6. Q) Q) Q) en en en '" o C. Q) en ... o C. Q) en I j "' o C. Q) en co o C. Q) en .... co o 0 6. 6. Q) Q) en en • '" o C. Q) en o ~ , a. Q) en 1.00E-11 1.00E-12 1.00E-13 ., ~ (/)1.00E-14 Ol o d 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCilml Pre 1994 MPC Limit = 4E-12uCilml Pre 1994 ALARA Goal = 1E-12 uCi/ml ~ 1\ 11 r , .!'.. J. -... *.J • It \. ~ '" (') ... LO to .... co (J) 0 co co co co co co co co co (J) , , , , , , , 6. 6. 6. a. a. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) ~ ~ ~ V~~ ~ '" (') (J) (J) (J) 6. 6. 6. Q) Q) Q) (/) (/) (/) BHV-2 Lead-210 Concentrations (uCi/ml) r • ... ~ J.. J .H1 I~ • ~ ... LO to .... co (J) 0 ~ '" (') ... LO to .... co (J) 0 (J) (J) (J) (J) (J) (J) 0 0 0 0 0 0 0 0 0 0 ~ , , , , , , , , , , 6. 6. 6. 6. 6. 6. , a. a. a. a. a. a. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) TAB 3 BHV-3 AIR SAMPLING GRAPHS AND DATA TABLE 1 Date 9/27/1982 1/3/1983 4/4/1983 1.74E-15 1.59E-15 1.76E-16 3.83E-16 1.91E-16 13/1984 h .OlE-16 -/2/1984 18.22E-16 7/2/1984 5.29E-16 10/1/1984 1.74£-16 1/2/1985 1.00£·17 '1/1985 1t.00£-16 '1/1985 11.04E-16 1.00E-16 2/1986 1.03E-15 1/1986 8.04E-16 ~.29E-16 6.45E-16 1.31E-16 3/16/1987 2.01£-16 2.16£-16 2.44E-16 .08E-16 '1811988 1.14E-16 '15/1988 2.08E-16 1.2lE-16 4.45£-16 1.05E-16 /1989 1.3lE-16 3/1989 1.67E- 114/1990 1/12/1990 /11/1991 /13/1";';11 '/1991 2/10/19 5/11/19 4.43E-16 3.84E-16 7.27E-17 .14E-17 1.41E-17 18.12E-17 n Limit: IBHV-3U I Effluent~ ALARAGoal ::: 12E-14 UCi/mI ISHV-3T 5E-13 uCi/ml n limit::. SHV-3R Effluent Concentration limit::: 6E-13 uCi/ml SHV-3PB ALARA Goal::. 1.5E-13 uCilm! 5E-12 uCi/m! Ipre 1994 MPC limit::: 18E-14 uCi/mll IPre 1994 MPC Limit::: 12E-12 uCi/ml IPro> lqq4 I\. '. ::: Pre 1994 MPC limit ::: 1.25 EFC EFC A Cone EFC EFC A Cone EFC EFC A Cone 5.ooE-12 1.25E-12 9.02E-16 8.ooE-14 2.ooE-14 2.87E-16 2.ooE-12 5.ooE-12 5.03E-16 1.30E-16 2.ooE-12 5.ooE-13 1.54E-14 5.ooE-13 2.25E-14 5.ooE-12 1.25E-12 5.25E-16 8.ooE-14 2.ooE-14 4.08E-16 2.00E-12 5.00E-12 1.25E-12 2.16E-16 8.ooE-14 2.00E-14 1.4lE-15 2.00E-12 5.00E-1311.96E-14 5.00E-13 2.40E-14 )E-12 1.25E-12 1.44E-15 8.00E-14 2.00E-14 5.36E-16 2.00E- .OOE-12 1.25E-12 1.23E-16 8.00E-14 2.00E-14 1.10E-16 2.00E-12 5.00E-l .00E-12 1.25E-12 6.94E-11 8.00E-14 2.00E-14 6.11E-17 2.ooE-12 5.00E-l .OOE-12 1.25E-12 9.59E-11 8.00E-14 2.00E-14 2.08E-16 2.00E-12 5.00E-13 5.00E-12 1.25E-12 3.05E-16 8.00E-14 2.00E-14 2.79E-16 2.00E-12 5.00E-13 [5.00E-12 1.25E-12 9.5lE-17 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-13 5.00E-12 1.25E-12 7.52E-16 8.00E-14 2.00E-14 5.20E-17 2.00E-12 5.00E-· 5.00E-12 1.25E-12 6.18E-16 8.00E-14 2.00E-14 1.40E-16 2.00E-12 5.00E-: 5.00E-12 1.25E-12 7.10E-17 8.00E-14 2.00E-14 1.00E-16 2.00E-12 5.00E-' .. 0IE-14 1.39E-14 l.70E-14 l.76E-14 9.17E-15 ,-14 .E-12 uCi/m! EFC EFC A ~.ooE-12 1.ooE-12 ~.ooE-12 l.ooE-12 )E-12 11.00E-12 )E-' .OOE-l ~.OOE-12 ~.OOE-12 ~.OOE-12 .00E-12 .OOE-12 .OOE-12 1.00E-12 l?OOE-12 1.25E-12 7.10E-17 8.00E-14 2.00E-14 7.80E-17 2.00E-12 5.00E-lill.73E-14 14.00E-12 [1.00E-12 15.00£-12 11.25£-1212.76£-16 18.ooE-14 12.00£-1414.10E-11 12.ooE-12 15.00E-13I1.12E-14 14.00£-12 11.00E-12 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 1.00£-16 2.00£-12 5.ooE-13 1.64E-14 4.00E-12 l.ooE-12 5.ooE-12 1.25E-12 1.ooE-15 8.ooE-14 2.ooE-14 1.00£-16 2.ooE-12 5.ooE-13 1.73E-14 4.00£-12 l.ooE-12 5.00£-12 1.25£-12 3.17E-16 8.ooE-14 2.ooE-14 1.25E-16 2.ooE-12 5.ooE-13 1.21E-17 4.00£-12 l.ooE-12 l?00£-12 1.25£-12 1.93E-17 8.ooE-14 2.ooE-14 1.54E-16 2.ooE-12 5.ooE-13 1.69E-14 4.ooE-12 l.ooE-12 5.00£-12 1.25£-12 1.77£-16 2.83E-16 1.97£-14 4.ooE-12 1.ooE-12 5.00£-12 9.89E-17 4.16E-15 1.64E-14 4.ooE- 5.00£-12 1.25E-12 O.ooE+oo 8.00£-14 2.00E-14 4.16E-17 2.00E-12 5.00£-13 4.6OE-15 4.ooE-12 l.ooE-12 5.ooE-12 1.20E-16 8.00£-14 2.00E-14 5.73E-17 1.6OE-14 4.ooE-12 1.ooE-12 5.ooE-12 1.96E-16 7.38E-17 1.59E-14 l.ooE-l- 5.ooE-12 2.18E-16 3.52E-17 1.46E-14 1.00E-12 5.ooE-12 2.32£-16 2.37E-17 2.48E-14 1.00E-12 5.00E-12 1.25E-12 2.55£-16 8.ooE-14 2.00E-14 3.42E-16 2.00E-12 5.00E-13 5.61E-14 4.00E-12 1.00E-12 5.00E-12 1.25E-12 4.14£-17 8.ooE-14 2.00E-14 1.00E-16 2.00£-12 5.00E-13 1.20E-14 4.00E-12 1.00E-12 5.00E-12 1.25E-12 3.06E-16 8.ooE-14 2.ooE-14 3.65E-17 2.ooE-12 5.ooE-13 1.36E-14 4.ooE-12 1.ooE-12 5.00E-12 1.25E-12 2.93E-16 8.ooE-14 2.00£-14 1.09E-16 2.ooE-12 5.00E-13 2.48£-14 4.00E-12 l.ooE-12 5.00E-12 1.25E-12 4.78E-17 8.00E-14 2.00£-14 2.47E-17 2.00E-12 5.00E-13 3.34E-14 4.00£-12 1.00E-12 5.ooE-12 1.25E-12 1.ooE-16 8.ooE-14 2.ooE-14 2.45E-17 2.ooE-12 5.00E-13 6.56E-15 4.00E-12 1.ooE-12 5.00E-12 1.25E-12 5.85E-17 8.ooE-14 2.ooE-14 3.97E-17 2.ooE-12 5.00E-13 6.75E-15 4.00£-12 1.ooE-12 )cE-12 1.25E-12 3.87E-17 8.ooE-14 2.ooE-14 8.03E-17 2.ooE-12 5.00E-13 1.69E-14 4.00£-12 1.ooE-12 5.ooE-12 l.ooE-16 3.50E-17 2.00E-12 5.ooE-13 2.3~14 4.ooE-12 1.ooE-12 5.ooE-12 2.54E-16 1.02E-16 5.ooE-13 1.68E-14 1.00E-l 5.ooE-12 2.87E-16 1.2lE-17 7.86E-15 1.ooE-12 5.ooE-12 1.25E-12 1.34E-16 8.ooE-14 2.00E-14 8.53£-17 2.ooE-12 5.00E-13 2.01E-14 4.00E-12 1.00E-12 5.00£-12 8.48E-16 1.94E-17 3.69E-14 1.00E-12 5.00E-12 7.40E-17 1.50E-14 1.00E-12 5.ooE·12 6.22E-17 1.77E-14 1.00E-12 5.00E-12 2.19£-18 1.18E-14 l.ooE-12 5.ooE-12 11.25E-12 2.35E-17 [8.ooE-14 2.ooE-14 [2.76E-18 2.ooE-12 5.ooE-13 3.57E-14 4.00E-12 1.ooE-12 L25E-12 5.80£-17 [8.ooE-14 2.00E-14 [3.36E-17 2.ooE-12 5.ooE-13 1.28E-14 4.ooE-12 1.00E-l: ~ ~~r -~ r OOE-12 j}.25E-l~.19E-17 ~.ooE-14 +2.ooE-l~.ooE-18 .+2.ooE-12 5.ooE-13 1.59E-14 4.00E-12 l.ooE-l .OOE:'; 4.ooE-17 2.68E-17 2.00E-14 1.07E-17 5.00E-13 1.8lE-14 '21911993 7.94E-17 1.00E-16 I.09E-16 2.69E-14 4.ooE-l 5/10/1993 1.6OE-17 5.00E-12 1.25E-12 5.07E-17 8.ooE-14 2.00£-14 7.64E-17 2.ooE-12 5.ooE-13 1.26E-14 4.ooE-12 1.ooE-12 8/10/1993 6.00E-17 5.ooE-12 1.25E-12 6.00E-18 8.ooE-14 2.00E-14 1.00E-16 2.CXIE-12 5.ooE-13 1.50E-14 4.00£-12 1.00E-12 11/8/1993 1.00E-16 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 1.00E-16 2.ooE-12 5.00E-13 2.10E-14 4.00E-12 1.00E-12 2/7/1994 1.6lE-16 5.ooE-12 1.25E-12 1.00E-16 8.ooE-14 2.ooE-14 2.22E-16 2.00E-12 5.00E-13 2.23E-14 4.ooE-12 1.00E-12 :5/9/1994 12.77E-16 15.ooE-12 11.25E-1212.8OE-17 18.00E-14 12.00E-1418.37E-18 12.ooE-12 15.00E-1311.40E-14 14.00£-12 [1.00£-12 7.39E-17 5.00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 1.14£-16 1.00E-12 9.05E-17 5.00E-12 1.25£-12 l.ooE-16 81911995 17.30E-17 19.ooE-14 b .25£-1419.20E-17 b .ooE-14 15.00£-1514.40£-17 19.ooE-13 b.25E-1311.96E-15 16.00£-13 11.50E-13 I Date 11/1995 '1996 /1996 i/1996 2/6/1997 5/5/1997 L1/1997 ;/1998 .0/1<><>0 '/2/2001 /2002 /2002 l2/3O/2002 1/31/2003 3/29/2004 6/27/2004 6/29/2005 9/26/2005 1/3/2006 /3/2006 /3/2006 12/31/2007 3/31/2008 1/1512009 ,Effluent 4 IALARA Goal = Limit = 19E-14 uCi/ml IBHv-3u limit: IBHV-3T IEffluent 4 :ALARA Goal: limit: 19E-13 uCi/ml IBHV·3R n Limit' IPre 1994 MPC limit: IPre 1994 ALARA GOAL::: .OOE-lj 16E-16 3.41E-16 l.31E-16 3.00E-16 li4IE-16 1.31E-16 3.16E-16 I.41E-16 U1E-16 ~.OOE-16 ~.41E-16 1.31E-16 3.ooE-16 3.16E-16 3.41E-16 1.31E-16 3.ooE-16 3.16E-16 3.41E-16 1.31E-16 3.00E-16 1.16E-16 3.41E-16 1.3lE-16 3.ooE-16 1.16E-16 3.41E-16 1.31E-16 3.ooE-16 3.16E-16 3.41£-16 1.31E-16 .ooE-16 3.16E-16 3.41E-16 l.3IE-16 .OOE-16 3.16E-16 3.4IE-16 1.31E-16 3.ooE-16 16E-16 Z.2SE-14 uCi/ml 11= ISE-12 uCi/mt I Pre 1994 MPC limit : ~.25E-12 uCi/ml IPre 1994 MPC limit = ~ GOAL: Z.2SE-13 uCi/ml 2E-12 uCi/ml 5E-13 uCi/mJ II: Pre 1994 MPC limit: IEFC IEFCA IEFC EFC A Conc EFC EFI :A ,. Pre 1994 j Conc __ IEFCA 14 ;-14 2.ooE-14 5.ooE-15 6.58E·17 9.ooE-13 2.25E 1'_14 ;-14 2.ooE-14 5.ooE-IS 1.18E-16 9.ooE-13 2.2SE-13 2.69E-14 16.ooE- .ooE-14 5.ooE-15 1.82E·16 9.ooE-13 2.25E·13..l..1.53E-14 .J!i.ooE-13 ..n..50E-13 :-14 12.25E-1413.43E-16 12.ooE-14 15.00E-15 13.99E-16 19.00E-13 12.25E-13 h .31E-14 16.ooE-13 h.50E-13 9.ooE-14 12.25E-14 h .31E-16 12.00E-14 15.00E-15 16.58E-17 19.ooE-13 12.25E-13h.91E-14 16.ooE-13 11.50E-13 9.ooE-14 1z.25E-141z.26E-16 I2.CXI£-14 15.00£-15 11.18£-16 19.00£-13 12.25E-13 12.69£-14 16.00£-13 h .50E-13 9.ooE-14 12.25E-14 1.39E-16 2.ooE-14 5.ooE-15 1.82E-16 9.ooE-13 2.25E-13 1.53E-14 6.00£-13 -!1.50£-13 9.ooE-14 12.25£-14 3.43E-16 2.ooE-14 5.00£-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-: U5E-14 1.31E-16 2.ooE-14 5.00E-15 6.58E-17 9.00£-13 2.25E-13 1.91E-14 6.ooE-13 1.50E-13 9.ooE-14 ~.25E-14 2.26E-16 2.ooE-14 5.ooE-15 1.18E-16 9.ooE-13 2.25E-13 2.69E-14 6.ooE-13 ..l..1.50£-13 .ooE-14 12.25E-14 1.39E-16 2.ooE-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53£-14 6.00E-13 1.50£-13 9.00E-14 12.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.3IE-14 6.00E-13 1.50E-13 KJE-14 -l.?-.25E-14 1.31E-16 2.00E-14 5.ooE-15 6.58E-17 9.ooE-13 2.25E-13 1.9IE-14 6.00E-13 1.50E-13 25£-14 2.26E-16 2.ooE-14 5.ooE-15 1.18£-16 9.ooE-13 2.25£-13 2.69E-14 6.ooE-13 1.50E-13 .ooE-14 2.25E-14 1.39E-16 2.00£-14 5.00£-15 1.82E-16 9.ooE-13 2.25E-13 1.53E-14 6.00£-13 1.50E-13 .OOE-14 2.25E-14 3.43E-16 2.ooE-14 5.ooE-15 3.99E-16 9.ooE-13 2.25E-13 1.31E-14 6.ooE-13 1.50E-13 .OOE-14 2.25E-14 1.31E-16 2.00E-14 5.ooE-15 6.58E-17 9.00E-13 2.25£-13 1.91£-14 6.00E-13 1.50E-13 9.ooE-14 2.25E-14 2.26E-16 2.00E-14 5.00£-15 1.18E-16 9.00£-13 2.25£-13 2.69E-14 6.ooE-13 1.50£-13 :-13 )E-13 19.ooE-14 12.25E-14 h .39E-16 12.ooE-14 15.ooE-15 h .82E-16 19.ooE-13 12.25E-1311.53E-14 16.ooE-13 11.50E-13 19.00£-14 12.25E-1413.43E-16 12.ooE-14 15.00£-15 13.99E-16 19.ooE-13 12.25£-1311.31E-14 16.00E-13 11.50E-13 9.00E-14 2.25E-14 11.31E-16 2.00E-14 15.00£-15 6.58E-17 9.00£-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 9.00E-14 2.25E-1412.26E-16 2.ooE-14 15.ooE-15 1.18£-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 ~.00£-14 +2.25E-l~.39E-16 -kZ.OOE-14 15.ooE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 I 1.50E-13 9.00E-14 2.25E-14 3.43E-16 2.00£-14 5.ooE-15 3.99E-16 9.00E-13 2.25E-l 9.ooE-14 2.25E-14 1.31E-16 2.00E-14 5.00£-15 6.58E-17 9.ooE-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.ooE-13 1.50E-13 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00£-15 1.82E-16 9.00E-13 2.25E-13 1.53£-14 6.ooE-13 1.50E-13 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00£-15 3.99£-16 ~I'_'":I' '''1'_'":1 , ":111'_1.1. J;tvll'_1"l 1 <;nl'_1"l I -11.50£-13 9.OOE-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.5SE-17 9.ooE-13 2.25E-13 1.91E-14 6.00E-13 L9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00£-15 1.lSE-16 9.ooE-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 1£-14 2.25£-14 1.39E-16 2.00£-14 5.ooE-15 1.82E-16 9.ooE-13 2.25E-13 1.53E-14 6.00£-13 1.50E-13 1E-14 2.25£-14 3.43E-16 2.ooE-14 5.ooE-15 3.99E-16 9.ooE-13 2.25E-13 1.3IE-14 6.ooE-13 1.50E-13 2.25E-14 1.31E-16 2.00E-14 5.ooE-15 6.58E-17 9.00E-13 2.25E-13 1.9IE-14 6.ooE-13 1.50E-13 .ooE-14 2.25E-14 2.26E-16 2.00£-14 5.00E-15 1.18E-16 2.25£-13 2.69E-14 6.ooE-13 1.50E-l: l tvll' '" "} "}<;1'_1" 1 ":I<>1'.1J; "} tvll'_1" <; tvll'_'" 1 R'I'_'~ 2.25E-13 1.53E-14 6.ooE-13 1.50£ ~. -_.DE-l' (Log Scale) ~ ~ ~ ~ ~ ~ ~ a a a a a a a 0 0 0 0 0 0 0 m m m m m m m , , , , , , , ~ ~ ~ ~ ~ ~ ~ 00 -.., 0> CJ1 ..,. W '" Sep-81 Sep-82 Sep-83 ..", .-I ~ " st 8 ~ Sep-84 Sep-85 + Sep-86 Sep-87 c :Ii ~ ".. ~ I I .? I I '" ~ t.. 7-I ~ ... ~ '" :::l Sep-88 c' 3 z Sep-89 '" C Sep-90 ~ Q!. + Sep-91 Sep-92 -l :::T 0 Sep-93 ~ c' ..:::: ~ ;: '-1 :::: :. I "-". ~ ~ ::. I • 3 Sep-94 , '" w 0 Sep-95 + Sep-96 ;JJ Sep-97 '" c. c' 3 Sep-98 , '" '" Sep-99 0> + Sep-OO r Sep-01 ct> '" c. Sep-02 , '" ~ 0 Sep-03 Sep-04 Sep-05 Sep-06 Sep-07 Sep-08 Sep-09 Sep-10 i'ljJ I I I k:: ~[:>4 I ~ ..... ... ~~ .t;P- '~ ~~ ~P- -~~ ~~ ~ L ~ ~~ ~ ~~ ~p. ~ ~~ r ~'~ ~p. ~ ~~ ~~ ~ ~~ ~p. ~ ~. .t:.,:;" ~~ .t:.,'>t 1 ~ ~,~ ~ --I. ... ~ . 1.00E-11 1.00E-12 1.00E-13 _1 .00E-14 '" ~ (f) C> a --' ~1 .00E-15 1.00E-16 1.00E-17 1.00E-18 ~ Effluent Concentration Limit = 9E-14 uCilml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml -.. -~ ~I IV \j If 'i V l~ - ~ N '" ... '" <0 r--<Xl '" a <Xl <Xl <Xl <Xl <Xl <Xl <Xl <Xl <Xl '" , , , , 6. 6. 6. 6. 6. 6. 0. 0. 0. 0. '" '" '" '" '" '" '" '" '" '" (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) I Ii ~ N '" '" , , 0. 0. '" '" (f) (f) BHV-3 Uranium-Natural Concentrations (uCi/ml) 11 -' Ii I I "tV III V I I II f '" ... '" <0 r--<Xl '" a ~ N '" ... '" <0 r--<Xl '" a '" '" '" '" '" '" '" a a a a a a a a a a ~ , , , , , 6. 6. 6. , , , 6. 6. 6. 6. , , , 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. '" '" '" '" '" '" '" '" '" '" '" '" '" '" '" '" '" '" (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) Sep-81 Sep-82 Sep-83 Sep-84 Sep-85 Sep-86 Sep-87 Sep-88 Sep-89 Sep-90 Sep-91 Sep-92 Sep-93 Sep-94 Sep-95 Sep-96 Sep-97 Sep-98 Sep-99 Sep-OO Sep-01 Sep-02 Sep-03 Sep-04 Sep-05 Sep-06 Sep-07 Sep-08 Sep-09 Sep-10 ~ a a m , ~ co - - ~ a a m , ~ ..." I ~ a a m , ~ 0> .., I> V'" I ...... ~ ... ~ 4 1:2~ i ~~ !~ ~ 1::2 ~ I ::2~ i :2~ .~~ .-::::: ::2 ~ 1 :2~ I ~~ ~~ '-::1- .-::~ :2~ ,+s~ '.-::::: ~ (Log Scale) ~ ~ ~ a a a a a a m m m , .'.... , ~ ~ en .... w - ~ a a m , ~ IJJ ::r -::: w -I :7 o :::!. c: 3 • N W o n o :J n CD :J .... a o· :J en ~ c: n ::.: 3 - Sep-81 Sep-82 Sep-83 Sep-84 Sep-85 Sep-86 Sep-87 Sep-88 Sep-89 Sep-90 Sep-91 Sep-92 Sep-93 Sep-94 Sep-95 Sep-96 Sep-97 Sep-98 Sep-99 Sep-OO Sep-01 Sep-02 Sep-03 Sep-04 Sep-05 Sep-06 Sep-07 Sep-08 Sep-09 Sep-10 ~ 0 a m , ~ 0> - - - - - ~ 0 a m .'.... "" , I , ~ 0 a m , ~ 0> 1.-:: ~ ~ ..... '-- ..... -..... ..... , ..... -..... -..... -..... ..... ..., ..... -..... -..... -:; .... ..., ..... -..... ..., ..... (Log Scale) ~ ~ ~ 0 0 0 a a a m m m , , , ~ ~ ~ '" .... w ~ 0 a m , ~ '" ~ OJ ::r ~ to) ::0 III Co c: 3 • N N Q) (") o :::J n (I) :::J .... i o· :::J en ~ c: Q -3 - 1.00E-11 1.00E-12 1.00E-13 Q) ~ Ul1 .00E-14 Cl 2. 1.00E-15 1.00E-16 1.00E-1 7 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCilml Pre 1994ALARA Goal = 1E-12 uCi/ml •.• 1\ 11: • ~I .. ~ 1 ¥~I ~ 'l' ~,.... V r, ~ N C') v 0{) CD "-co C) 0 co co co co co co co co co C) a. a. a. a. a. a. a. a. a. , a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Ul Ul Ul Ul Ul Ul Ul Ul Ul Ul ~ .... ~~~ ~ N C') C) C) C) , a. a. a. Q) Q) Q) Ul Ul Ul BHV-3 Lead-210 Concentrations (uCi/ml) Jf.. J\ ~ 1'1 1'1 1'1 1'1 .Jf.. 1'1 J\ J\ . fI.. 1'1 7.. 1'1 vv _VVV VVVVVV VVV ~ ~ v 0{) CD "-co C) 0 ~ N C') v 0{) CD "-co C) 0 C) C) C) C) C) C) 0 0 0 0 0 0 0 0 0 0 ~ a. a. a. a. a. , a. , , , a. a. a. a. a. a. , a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Ul Ul Ul Ul Ul Ul Ul Ul Ul Ul Ul Ul Ul Ul Ul Ul Ul TAB 4 BHV-4 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Umit = 9E·14 uCi/ml BHV-4U Effluent Concentration limit = 2E-14 uCi/ml BHV-4T Effluent Concentration limit = 9E·13 uCi/ml BHV-4R ALARA Goal = 2.25E·14 uCi/ml ALARA Goal = 5E-13 uCi/ml ALARA Goal = 2.25E·13 uCi/ml ALARA Goal = .. r." ..... :, , "-_.""',, .. "' ... ,: :.-.. " ........ ,' , Pre 199-'Pre 1994MPC Umit= 15E-12uCi/ml Pre I9~ •• " .. ~"" .. _ .... -.. _ ..... ,,,,, .,"' ...... _ ...... I\. GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre ~94 j ~ 5.20E- 4.5.'l.I'- -kEFC EFC A Cone EFC EFC A Cone EFC EFC A Cone 15.00E-12 1.25E-12 2.93E-15 8.00E-14 2.00E-14 2.74E-15 2.00E-12 5.00E-13 1.84£-14 ~00£-12 1.25£-12 1.78E-15 8.00E·14 2.00E-14 2.29E-15 2.00E-12 5.00E-13 2.54£-14 --.--------------------------07E- 1.57£·14 2.00E-14 L26£·14 7.58£-16 1/3/1983 14.33E-15 6.52E-16 E-14 8.00E-14 8.00E-14 2.00E-14 5.35E-15 2.00£-14 6.04E-16 1.25E-15 7.17E-: 3.73E-16 5.00E-12 1.25E-12 9.43E-: 2.54E-16 5.00£-12 1.25£·12 1.51E-l E-14 :-14 )()£-14 16.76£-16 .00£·14 14.13E-16 2.65E- 11/3/1984 12.76E-15 ]5.ooE·12 ]1.25E-12 11.60E~~ OE-14 )()E-1411.0SE-lb 14/2/1984 14.27E-16 15.ooE·12 11.25E-12 12.33E-16 .ooE-14 2.ooE-1416.28E-16 /1984 12.57E-15 15.00£-12 11.25E-12 !t.36E-16 8.ooE-14 8.00£- 2.00E-14 1.11£-16 £-14 1.10£-17 L25E- /1985 15.30E-17 15.00E-12 11.2sE-lZ 13.5St-1l .ooE·14 2.00£·14 17.00£-18 /1985 11.00£-16 ]5.00£-12 11.25£-12]6.00£-16 ~OOE·14 2:OO.~-14 14.35E-17 17/1/1985 19.36E-16 15.00£-12 h .25E-12 12.33E·16 .00£·14 2.ooE-1412.36E-16 ~/30/1985 11.46E.15 5.00E-12 1.25E-12 ]7.69£-: :-14 :>£-1415.38£-16 " 1/2/1986 8.40£-15 5.00E-12 1.25E-l "/1/1986 15.79£,15 5.00£-12 1.25E-1215.80E.l .. 00£-14 .OO~ 1E-14 -1412.99E-16 ;.19£·15 5.00E-12 1.25E-12 7.83E-ll [)E-1412.20E-15 4.60E-15 5.ooE-12 1.25E-12 4.67£-16 8.00E-14 2.75E-15 5.00E-12 1.25E-12 5.9OE·16 8.00E-14 6/1987 4.64E-15 5.00E-12 1.25£-12 1.18E-IS 8.00£-14 2.00£-14 2.37E-15 2.ooE-14 9.39E-16 2.00£-14 4.97E-16 1/1987 4.35E-15 5.00£-12 1.25£-12 1.23£-14 8.00£·14 2.00£-14 1.13E-15 2.00£-14 2.26E-: .00£-14 2.20E-15 1/1987 6.39E-15 5.00£-12 1.25£-12 1.50E-14 8.ooE-14 5.72E-15 5.00£-12 1.25E·12 4.53E-16 ___ _ 8.QC1~-14 1.91E-15 5.00£-12 1.25E-12 1.35E-14 8.ooE-14 2.00E-14 4.42E-16 2.00E-14 4.92£-: 2.00£-14 1. 1s/18/1988 1.78E-14 5.00E·12 1.25E-12 4.39E-14 8.00£-14 8/15/1988 7.56E-15 5.00£-12 1.25£-12 3.31E-14 8.00E-l ·1/1.d/1QAA 1.47E·14 5.00£-12 1.25£-12 1.56E·15 8.00E·14 2.47E·15 15.00£,12 11.25E-12 13.14£.15 8.00£·14 2.ooE·14 6.94E-l '14/1989 1/13/1989 2.50E-16 -#.OOE-12 -4r25E-lw .68E-15 8.00E-14 2.00£-14 9.03E-16 8.00E-14 2.00£-14 2.35£·15 1.92£-15 2.91£-15 1.67E-16 1.87E-16 U5E-1I 1.77E-16 1.83E-16 4.40E-16 909E·17 11/9/1992 2.07£-16 2/9/1993 1.73E- 5/10/1993 2.70E- DE-17 1.00E-16 12/7/1994 [1.10£-16 5/9/1994 8/9/1994 1117/1QQ{ 1.45E-16 5.00£-12 5.ooE-12 .00E-: .00£-: . OOE-: .ouE-l 5.00E-12 5.00£-: 5.00£-12 5.ooE-12 5.00£-12 5.00£-12 .00E-12 .OOE-· 3£-14 9.ooE-14 9.00E-14 "l!> 8.00E-14 2.00E-14 4.03E-15 :-15 8.ooE-14 2.00£-14 2. :·15 8.ooE-14 2.00E-14 2.33E-15 1.25E.l~.87E-15 8.ooE-14 2.00E-14 5.06£-16 .. 25£-1212.25E-17 8.ooE-14 2.00E-14 1.08E-15 l!:25E-IU!.89E-16 8.00£-14 2.00E-14 6.38E·17 1.25£-12 2.6IE-15 8.00£·14 2.00E-14 3.54E·16 1.25E-12 4.38E-16 8.00£-14 2.00E-14 1 . 1.25£-12 1.46E-16 8.00£·14 2.00E-14 3.76E·17 1.25E-12 1.95£-15 8.00E-14 2.00E-14 1.33£-16 ,.25£-12 2.56E-16 8.00£-14 2.ooE-14 4.04E-16 •. 25E-12 1.15£·16 8.00E-14 2.00E-14 4.50E-17 1.25E-12 1.ooE-16 8.00£-14 2.ooE-14 3.62£- 1.25£-12 2.76E-17 8.00£-14 2.ooE-14 2.89E- 1.25E·12 2.50E-17 8.00£-14 2.00E-14 8.74E- l.25E-12 1.76E-16 8.00E-14 2.00£-14 0.00£+00 l.25E-12 1.00E-16 6.ooE·17 l.25E·12 3.38E-16 2.2IE-16 :-14 1.25E·14 2.86E-16 1.25E-14 2.31£-15 8.00£-14 8.00£·14 .00£-14 .00£-14 5.00E-l~ .ooE-14 5.00£-1517.10E-17 2.00E·12 2.00E·12 2.ooE-12 2.ooE-" l.00£·12 2.00£-12 2.00E-12 2.ooE-I' 2.ooE-12 2.ooE-12 2.00£-12 2.00E·12 2.00£·1; 2.00E-12 2.00E·12 2.00E·12 2.00£-12 2.00E·1 2.00£·12 2.00E-12 .00E-12 .00E-12 t.ooE .00' .00E-12 2.00E·12 2.00£-12 2.00E-12 2.00£-12 [2.ooE-12 2.00E-12 2.00E-12 12.ooE-12 9.00E-13 -1' .ooE-1312.57£~ 5.00£-1312.00£·14 5.00E-13 1.20E-14 5.ooE-13 2.50E-: .UUt-B 11.59£-16 .00E-13 13.67£-14 5.00£·13 11.58£-14 5.00£·13 9.83£-15 5.ooE-13 2.57E-14 .ooE-13 15.02E-15 5.00E-13 17.48£-15 5.00£·1317.86E·15 2.12E-14 1.33E-14 1.13E-14 1.20E-14 5.89£·14 5.00E-13 12.21£-14 5.ooE-: 1'S':ilOE-"1312.55E-14 15.00£-13 4.44E-14 )£-13 1.38E-14 .00£·13 1.97E-14 .OOE-: 2.12E-14 8.0SE-15 9.95E·15 E-14 1£-13 8.86E-15 5.00£-13 2.19£-14 5.00£·13 4.19E-14 .40£-14 ~5£-14 5.00£-13 1.41E-14 5.00E-13 1.57t.!!. :-14 :-14 :-14 5.00E·13 1.75£-14 5.ooE-13 3.08£-14 5.ooE·13 11.73E-14 t.25E-1312.70E-15 limit = 16E-13 uCi/ml ISHV-4PB 1.5E-13 uCi/ml uCi/ml IEFC IEFC A 4.00E-121.ooE-12 4.00E-12 h .OOE-12 4.00E-12 l .ooE-12 4.ooE-12 l .ooE-12 -.00E-12 1.00£-12 .00E-12 1.00E·12 .00E-12 11.ooE·12 4.00£-12 1.00£-12 4.ooE-12 1.00£-12 .. 00£·12 1.00£·12 .00£·12 ]1.00£·12 4.00£·12 11.00£-12 4.ooE·12 1.ooE·12 4.ooE-12 1.00E-12 -.OOE-12 1.00E-12 4.00£-12 11.00E-12 4.00E-12 11.00E-12 1.00E·12 4.00E·12 1.00E·12 4.ooE·12 1.00E·12 4.00E-12 1.00£-12 4.00E·12 1.00E-12 4.00E·12 1.00£·12 4.00E-12 l.ooE-12 4.00£-12 1.00£-12 4.00£-12 l.ooE-12 4.00£·12 1.00£·12 4.00E-12 1.00E·12 4.00E-12 1.00E-12 4.00£-12 1.00E-12 4.ooE-12 l.ooE-12 4.00£-12 1.00£-12 II..00E·12 1.00£·1; ~.ooE·12 ~.OOE·12 4.00E-12 4.00E-12 11..00£- :l£-1 4.00£·12 4.00E-l: 4.00£-1; 1.00£·12 1.00E-12 .OOE-12 .OOE-12 00£·12 .00£·12 1.00£-12 1.00E-12 I Date 2/5/1996 5/6/1996 IEffluent I ALARAGoal = Pre 1994MPC = 9E-14 uCi/ml 8HV-4U Effluent Concentration limit = 2E-14 uCi/ml 8HV-4T Effluent Concentration limit = 19E-13 uCi/ml 18HV-4R 1 Effluent Concentration Limit = 16E-13 uCi/ml IBHV-4P8 2.25E-14 uCi/ml ALARA Goal = 5E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml l kALARA Goal = ....u. ... j:-., ..... :1_. 5E-12 uCi/ml Pre 1994 MPC limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml . :f'i ~LAI{A bURl. = Pre 1994 ALARA GOAL = _~j:_t7"(,i/ml Pr"1~ ... _. --- Cone Cone Cone EFC A 1.43E-14 5.70E-15 2.61E-15 5.6OE-15 1.50E-13 1.19E-14 3.80E-16 6.10E-15 6.48E-15 16.ooE-13 11.50E-13 4.55E-16 3.57E-15 2.84E-16 9.ooE-13 2.25E-13 7.68E- 9.ooE-13 2.25E-13 4.90E-15 1.50E-13 1.36E-15 I.00E-16 1.10E-14 1.50E-13 1216/1997 11.oo£~16 1.40E-16 1.03E-16 6.76E-15 1.50E-13 15/5/1997 1.00£-16 9.00E-14 2.25E-14 4.ooE-16 2.ooE-14 5.00£-15 2.24E-16 9.00E-13 2.25E-13 4.55E-15 6.00E-13 1.50£-13 8/11/1997 4.74£-16 9.00E-14 2.25E-14 9.07E-16 2.00E-14 5.00£-15 1.00E-16 9.ooE-13 2.25E-13 5.55£-15 6.ooE-13 1.50£-13 1/5/1998 8.31E-16 9.ooE-14 2.25£-14 4.82E-16 2.00E-14 5.00£-15 1.77E-16 9.00E-13 2.25E-13 5.28E-15 6.ooE-13 1.50£-13 V28/1998 3.32E-16 9.ooE-14 2.25E-14 4.43E-15 2.00E-14 5.ooE-15 1.21E-16 9.ooE-13 2.25E-13 7.43E-15 6.ooE-13 1.50E-13 3/29/1999 7/3/1999 9/26/2000 12/26/2()()( 4.6OE-16 9.ooE-14 2.25E-14 9.02E-16 2.ooE-14 5.ooE-15 3.54E-16 9.ooE-13 2.25E-13 6.91E-15 6.ooE-13 1.50E-13 4.08E-16 9.ooE-14 2.25E-14 4.93E-16 2.ooE-14 5.ooE-15 2.53E-16 9.ooE-13 2.25E-13 4.52E-15 6.ooE-13 1.50£-13 7.72E-16 9.ooE-14 2.25E-14 3.75E-16 2.ooE-14 5.ooE-15 3.43E-16 9.ooE-13 2.25E-13 6.73E-15 6.ooE-13 1.50E-13 5.11E-16 9.ooE-14 2.25E-14 4.70E-16 2.ooE-14 5.ooE-15 3.70E-16 9.ooE-13 2.25E-13 8.96E-15 6.ooE-13 1.50E-13 9.ooE-14 2.25E-14 9.89E-16 2.ooE-14 5.ooE-15 1.28E-16 9.ooE-13 2.25E-13 6.40E-15 6.ooE·13 1.50E-13 1.70E-15 9.00E-14 2.25E-14 7.SOE-16 2.ooE-14 5.ooE-15 4.61E-16 9.00E-13 2.25E-13 7.86E-15 6.ooE-13 1.50E-13 1.03E-15 9.ooE-14 2.25E-14 7.SOE-16 2.00E-14 5.ooE-15 2.43E-16 9.ooE-13 2.25E-13 6.42E·15 6.ooE-13 1.50E-13 1.00E-16 9.00E-14 2.25E-14 2.13E·16 2.ooE·14 5.00E-15 2.20E-16 9.ooE-13 2.25E-13 5.61E-15 6.ooE-13 1.50E-13 E-14 2.25£-14 3.08E-16 2.ooE-14 5.ooE-15 1.11£-16 9.ooE-13 2.25£-13 3.92E-15 6.00£-13 1.50E-13 .00E-l 2.25E-14 2.01E-16 2.00£-14 5.ooE-15 2.24£-16 9.ooE-13 2.25£·13 7.79E-15 6.00E-13 1.50E-1'" 2.25" ". ------OE·14 2.25E-14 1.ooE·16 2.ooE-14 5.00E-15 4.35E-16 9.00£-13 2.25E-13 8.45£·15 6.ooE-13 1.50E-13 OE-14 2.25E-14 1.00E·16 2.ooE-14 5.00E-15 1.ooE-16 9.00£-13 2.25E-13 6.37£·15 6.ooE-13 1.50E-13 '/2/2001 11.ooE-16 9.00E-14 2.25£-14 1.05E-16 2.ooE·14 5.ooE-15 1.ooE-16 9.00£-13 2.25E-13 6.99£-15 6.ooE-13 1.50E·13 1.91E-16 9.ooE-14 2.25£-14 1.00E-16 2.ooE-14 5.ooE·15 2.01E-16 9.ooE-13 2.25E-13 8.04£-15 6.00£·13 1.50E·13 2/31/2001 9.ooE-14 2.25£-14 2.05E-16 2.00E-14 5.ooE-15 l.ooE-16 9.ooE-13 2.25E-13 1.83£-15 6.00£·13 1.50E·13 /1/2002 2. !:J.OOt-14 1.25E-14 3.38E-16 2.00E-14 5.ooE-15 1.26E-16 19.ooE-13 !2.25E-1li7.48E-15 16.00E-13 11.5OE-13 '1/2002 1.97E-16 2.30E-16 1.ooE-16 9.ooE-14 2.25E-14 4.10E-16 2.ooE-14 5.00E-15 I.00E-16 19.00E-13 2.25£-13 7.40£-15 9.00E-14 2.25E-14 2.42E-16 2.00E-14 5.00£-15 1.56E-16 ~.OOE-13 -+.2.25E-14.4.21E-15 9.ooE-14 2.25E-14 1.92E-16 2.00E-14 5.00E-15 1.00£-16 ,., 1.' 1., E-14 2.25E-14 1.69E-16 2.ooE-14 5.ooE-1511.29E-16 19.ooE-13 12.25E-13 14.55E-15 16.ooE-1 .. OOE-15 ·15 6/30/2003 1.ooE-16 9.ooE-14 2.25E-14 2.87E-16 2.ooE-14 5.ooE 9/29/2003 1.00E-16 9.ooE-14 2.25E-14 8.53E-16 2.ooE-14 5.ooE-15 3.32E-16 ~.OOE-13 2.25E·13 8.69E-15 6.ooE-13 1.50E-13 12/29/2003 1.02E-16 19.00E-14 2.25E-14 1.00£-16 2.ooE-14 5.ooE-15 1.49E-15 9.00£-13 2.25E-13 9.45E-15 6.ooE-13 1.50£-13 00£-16 9.ooE-14 2.25E-14 1.26E-16 2.ooE-14 5.ooE-15 1.ooE-16 9.ooE-13 2.25E-13 2.00E-15 6.00E-13 1.50E-13 1.00E-16 9.ooE-14 2.25E-14 2.53E-16 2.00E-14 5.00E-15 1.ooE-16 9.ooE-13 2.25E-13 3.23E-15 6.ooE-13 1.50E-13 l.ooE-16 9.00E-14 2.25E-14 1.15E-16 2.ooE-14 5.ooE-15 1.ooE-16 9.ooE-13 2.25E-13 9.68E-15 6.00E-13 1.50E-13.J 12/27/2004 1.00E-16 9.ooE-14 2.25E-14 2.30E-16 2.ooE-14 5.ooE-15 1.ooE-16 9.ooE-13 2.25E-13 1.37E-14 6.ooE-13 1.50E-13.J 3/28/2005 1.00£-16 9.ooE-14 2.25E-14 2.66E-16 2.ooE-14 5.00E-15 3.15E-16 9.00E-13 2.25E-13 9.22E-15 6.00E-13 1.50E-13.J 6/29/2005 1.47E-16 9.ooE-14 2.25E-14 1.45E-15 2.ooE-14 5.ooE-15 1.42E-16 9.00E-13 2.25E-13 9.34E-15 6.ooE-13 1.5 9/26/2005 2.01E-16 9.ooE-14 2.25E-14 2.06E-16 2.ooE-14 5.ooE-15 4.80E-16 9.00£-13 2.25E-13 2.12E-14 6.ooE-13 1.5ut-13 1 1/3/2006 4.54E-16 9.ooE-14 2.25E-14 1.24E-16 2.ooE-14 5.ooE-15 1.ooE-16 9.ooE-13 2.25E-13 3.60£-14 6.ooE-13 1.50E-13 4/3/2 __ _ ~~ , QOt,~ 9.ooE-14 2.25E-14 1.32E-16 2.00E-14 5.ooE-15 1.00E-16 9.ooE-13 2.25E-13 8.36E-15 6.ooE-13 1.50E-l"!J 7/3/2006 2.76E-16 2.63E-16 1.ooE-16 1.03E-14 1.50E-13 10/2/2006 4.97E-16 9.ooE·14 2.25E-14 2.37E-16 1.00E-16 1.60E-14 1.50£-13 1/.007 16.46E-16 19.00E-14 12.25E-1412.81E-16 12.ooE-14 15.ooE-1511.ooE-16 19.ooE-13 12.25E-1312.10E-14 '/2007 7.08£-16 2.25E-1413.20E-16 12.00£-14 15.ooE-1511.ooE-16 '/2007 9.41E-16 2.25E-l< 3.30£-16 2.25E-14 1.42 E-15 2.25E-14 1/2008 9.00£-13 0/2008 3.6lE-16 9.ooE-13 0/2008 E-14 2.25E-14 9.ooE-13 9.ooE-14 2.25E-14 2.ooE-14 15.00£-15 1 19.ooE-13 1.56E-15 9.ooE-14 2.25£-14 4.57E-16 2.00E-14 15.ooE-15 2.99E-16 9.ooE-13 5.67E-17 9.ooE-14 2.25E-14 2.17E-16 2.ooE-14 -l?ooE-1~-+'1.51£-16 ~.ooE-13 2.25E-1 U5E-l U5E-l 2.25E-1 ~ 6.00£-13 1.50E-13 .18E-14 6.ooE-13 1.50E-13 6.ooE-13 1.50£-13 6.ooE-13 11.50E·13 4.05E-15 9.00£-14 82/15/2009 6.50E-15 9.00£- 2.25E-14 USE-IS 2.ooE·l. 2.25E-14 3.48E-16 2.ooE·14 15.00E-1511.33E-16 19.ooE-13 L.L;Jo:;-.d p ...... ",-."" 11.;Juo:;·."" Date Effluent Concentration limit = 9E-14 uCi/ml BHV-4U Effluent Concentration limit = 2E-14 uCi/ml BHV-4T Effluent Concentration limit = 9E-13 uCi/ml BHV-4R Effluent Concentration limit = 6E-13 uCi/ml BHV-4PB ALARAGoal" 2.2SE·14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal" 2.2SE-13 uCi/ml ALARAGoal = I.SE-13 uCi/ml Pre 1994 MPC limit" SE-12 uCi/ml Pre 1994 MPC limit" 8E-14 uCi/ml Pre 1994 MPC limit = 2E-UuCi/ml Pre 1994 MPC limit" 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL" SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 3/31/2010 6.01E-lS 9.00E-14 2.2SE·14 l.26E-16 2.00E-14 S.OOE-15 1.34E-16 9.00E-13 2.2SE-13 1.19E-14 6.00E-13 I.S0E-13 6/30/2010 2.33E-IS 9.00E-14 2.25E-14 7.29E-16 2.00E-14 S.OOE-15 2.66E-16 9.00E-13 2.2SE-13 3.27E-IS 6.00E-13 1.S0E·13 9/30/2010 4.77E-IS 9.00E-14 2.25E-14 1.80E-IS 2.00E-14 S.OOE-15 8.23E-16 9.00E-13 2.2SE-13 S.l1E-15 6.00E-13 1.50E-13 12/31/2010 3.93E-lS 9.00E·14 2.25E·14 3.90E-16 2.00E-14 S.OOE-lS 2.S6E-16 9.00E-13 2.25E-13 1.13E-14 6.00E-13 1.SOE-13 UI r::: o :;::; E -r::: GI () r::: o o GI :E '0 ::::J r::: .2 '0 ~ "'" ::> J: III N '" ~ ~ , , w w 0 0 '" '" ~ I'" • r--. < ~ 4 "'"'4 ~ "' ... ) : • ~ ..:: 4 ~ ~ s;: I """ ~ ;>+ "!i: ..,. ~ , w 0 '" ~ 1lI ~ o~-das ~ 1 60-daS BO-daS LO-daS ~ ;;:1 90-daS 90-daS -." +c vO-daS £o-das 0 ~ -«:, ~ ~ ~ zo-das N , "0 '" ~o-das Q) --' OO-daS t I~ ... -,.., 66-daS CD N N ~ :£' .... ~ B6-daS , E .;2 L6-daS "0 '" OC 96-daS t 96-das 0 ~ ,. rr '" v6-das N , E £6-das .;2 0 .c l6-das l- t ~6-das 06-daS ro ~ ::J t: I Cii 6B-daS z E BB-das ::J .1" l'! --.... LB-das :J t 9B-das 9B-daS I vB-das ~ £B-das ~ lB-das ~B-das lO <D ..... 0() ~ ~ ~ ~ , , , , w w W W 0 0 0 0 '" '" 0 '" ~ ~ ~ ~ (ale~s 601) 1.00E-11 1.00E-12 1.00E-13 Q) ro () en1.00E-14 C) o d 1.00E-15 1.00E-16 1.00E-17 -'l - ~ co , a. Q) en Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCilml Pre 1994 MPC Limit = SE-12uCilml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml t J ':...~ - -'--' • -'---- - l I .,.. ... N O"J .... '" co .... co 0> a ~ co co co co co co co co 0> '" 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) en en en en en en en en en en ,~ N O"J .... '" '" '" 6. 6. 6. Q) Q) Q) en en en BHV-4 Uranium-Natural Concentrations (uCi/ml) -~ ¥ 1 t -f'-t l-f. _t lV" *--- If VI .~ I '" co .... co 0> a ~ N O"J .... '" co .... co 0> a '" '" '" '" '" a a a a a a a a a a ~ 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. 6. , , , a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) en en en en en en en en en en en en en en en en 1.00E-11 1.00E-12 1.00E-13 Q) ro " (/)1.00E-14 Ol o -='- 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 2E-14 uCi/ml ALARA Goal = SE-13 uCi/ml BHV-4 Thorium-230 Concentrations (uCi/ml) Pre 1994 MPC Limit = 8E-14uCi/ml ~ ,.. \1 II • • ~ .... W¥ ~ N ~ ~ N '" co co co 6. 6.. 6.. Q) Q) Q) (/) (/) (/) ~ ~ ~ ID ~ ro rn a ~ N M ~ ~ ~ ~ ro ro ro ro ro ro rn rn rn m m rn rn rn I I I , I I I I I I I I I I ~ ~ ~ ~ ~ ~ n ~ n n n n n n m m m ~ m m m w W W ID ID ID ID (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) (/) co CJ) , a. Q) (/) CJ) CJ) , a. Q) (/) ¥\ L ... T t." ~\ \~ o o , a. Q) (/) ~ o , a. Q) (/) ... N o , a. Q) (/) I)¥ \J ~ '" o 6. Q) (/) .... o 6. Q) (/) L() o 6. Q) (/) '" o 6. Q) (/) .... co o 0 6.. 6. Q) Q) (/) (/) CJ) 9 a. Q) (/) II ~ o ~ , a. Q) (/) 1.00E-11 1.00E-12 1.00E-13 ~1 .00E-14 Q) ro u CfJ 0> o -' ~1 .00E-15 1.00E-16 1.00E-17 1.00E-18 Effluent Concentration Limit = 9E-13 uCilml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml r. .. .. .~ v. • I / '! ~ N (") " 10 co "-co 0> a co co co co co co co co co 0> , 6. 6. 6. 6. 6. 6. 6. , , 0. 0. 0. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ 4 ~ 1 ~ N (") 0> 0> 0> , , , 0. 0. 0. Q) Q) Q) CfJ CfJ CfJ BHV-4 Radium-226 Concentrations (uCi/ml) \ tM~ .t • I~ _[~_ 1\ -tr-; • Ij~ J\AAA ¥ A ¥ .. " 10 co "-co 0> a ~ N (") " 10 co "-co 0> a 0> 0> 0> 0> 0> 0> a a a a a a a a a a ~ , , , , , , , , , , 6. 6. 6. 6. 6. 6. , 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ CfJ 1.00E-11 1.00E-12 1.00E-13 (j) ro <.:J OJ1 .00E-14 0) o --' 1.00E-15 1.00E-16 1.00E-17 ~ co , a. OJ OJ Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1E-12 uCi/ml t 7>.J. ¥ i\ ~ ¥ J N ('") .... '" CD "-co '" a co co co co co co co co '" , 6. , , , , 6. , , a. a. a. a. a. a. a. OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ .. " 1\ ~~ "V ~ N ('") '" '" '" , , , a. a. a. OJ OJ OJ OJ OJ OJ BHV-4 Lead-210 Concentrations (uCi/ml) ~ .. ~/ f'* • •• .... V V .... '" CD "-co '" a ~ N ('") .... '" CD "-co '" a '" '" '" '" '" '" a a a a a a a a a a ~ , , , , , , 6. 6. 6. 6. 6. 6. 6. 6. 6. , , a. a. a. a. a. a. a. a. OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ OJ TABS BHV-S AIR SAMPLING GRAPHS AND DATA TABLE I Date Pre 1994 MPC Umit = Pre 1994, 2.44E-15 U4E-15 1.04E-15 3.61E-15 1/27/1982 1.71E-14 /3/1983 1.90E- /4/1983 n Umit: 1.25E- EFC ,.00E-12 ,.00E-12 ,.OOE-12 ,.OOE·12 5.00E-12 5.00E- -;.OOE-12 7.62E·16 5.00E-12 4.86E-16 5.00E-12 1/1984 6.96E-15 5.00E-12 14/211984' '11:64E~i5 15.00E-12 7/211984 1.12E-15 5.00E-l IE-IS 15.OOE-12 ./2/1985 17.32E-165.00E-12 /1985 ]2.36E-16 5.00E-12 7.58E-16 5.00E- 7.47E-15 5.00E·12 1.75E-14 5.00E·12 2.99E-14 5.00E-12 5/30/1986 2.23E-14 5.00E-12 10/27/1986 2.33E·14 5.ooE-12 --.--.----5.00E- :-14 2.50E·14 19/9/1987 ]2.65E-14 1.80E-14 1.01E-14 5/18/1988 1. 78E- 9E-14 11/14/198814.46E-14 1.67E-14 2.03E-14 2.8lE·15 >.38E-14 4.48E-14 2.18E-14 18/13/1990 19.53E-15 - -'-2/1990 /1991 1'--"" "' 11991 1.22E-15 7.84E-16 >.37E-16 3.54E-16 1s7ii/1992 14.71E-16 8/10/1992 5.32E-15 '1/9/1992 3.66E-16 '9/1993 2.05E-16 4.8OE-16 a.30E-16 ~12.70E-16 1994 1994 1.OUt.-.L::I 1994 2.67E-15 9.21E-17 12/7/1995 1."5i"E-iS 5/9/1995 2.2lE-16 18/9/1995 ]1.66E-16 !!l.OOE-12 5.00E-12 5.ooE-12 5.00E-12 5.00E·12 5.00£-12 5.ooE-12 5.ooE-12 5.ooE·12 5.00E- 5.00E-12 5.00E-12 5.00E-12 5.00E-12 5.ooE-12 5.ooE-1: 5.ooE- 5.00E-12 5.ooE-12 .. 00E-12 ,.OOE-12 ·.ooE-12 )E-1 ;.OOE-12 9.00E-14 9.00E-14 ]9.00E-14 15E-13 uCi/ml 11 = BHV-5U Effluent I ALARAG Pre 1~ EFC A Cone IEFC A Pre 1994 MPC Limit = Pre 1994 ALARA GOAL = Com 1.25E·l 1.25E-12 2.78E-15 1.25E-12 2.62E-15 8.00E-14 2.00E-14 1.11£-15 1.25E-12 7.61E-15 8.00E-14 2.00£-14 1.39E-15 1.25E-12 9.46E-15 8.00E-14 2.00E-14 3.80E-15 1.25£-12 5.77£-15 8.ooE-14 2.00E-14 9.34E-17 1.25E-12 2.33E-15 8.00E-14 2.00E-14 5.93E-: 1.25E-12 3.25E-15 b.lHt-1!l 1.25E-12 1.1OE-15 3.63E-16 ~.25E-12 9.69E·16 9.60E-16 l.25E-12 1.34E-15 3.88E-15 1.25E-12 1.92E-15 8.ooE-14 2.ooE-14 3. 1.25E-12 3.13E-16 4.l1t-1b l.25E-12 6.71E-16 4.94E-16 l.25E-12 5.43E-16 2.71E-16 1.25E-12 4.00E-16 8.00E-14 2.00E-14 6.90E-16 1.25E·12 1.16E-15 8.00E-14 2.00E-14 2. 1.25E-12 7.24E-15 3,1Ut-1!l l.25E-12 7.64E-15 1.51E·14 l.25E-12 15.19E-15 8.00E-14 2.ooE-14 1.05E-14 l.25E-12 7.78E-15 8.00E-14 2.00E-14 1.60E-14 5.35E-15 8.ooE-14 2.00E-14 1.47E-14 ~.50E·15 8.00E-14 2.00E-14 6. l.25E-12 8.54E-15 !!.1!lt-1!l l.25E-12 6.62E-15 9.34E-15 l.25E-12 7.09E-15 7.20E-15 U5E-12 ]2.98E-15 L.25E-12 1.49E-14 U5E-12 1.39E-14 1.17E-14 U5E-12 5.54E-15 7.20E-15 U5E-12 7.05E-15 3.78E-15 8.00E-14 2.00E-14 9.26E-15 L.25E-12 8.0lE-15 8.00E-14 2.00E-14 1.81E-14 L.25E-12 1.48H4 8.00E-14 2.00E-14 1.28E-14 U5E-12 1.70E-14 8.00E-14 2.00E-14 1.59E-14 U5E-12 1.70E-14 8.00E-14 2.00E-14 3.27E-15 U5E-12 5.27E-15 8.00E-14 2.00E-14 5.38E- U5£-12 3.13E-16 8.00E-14 2.00E-14 2.3lE- U5E-12 6.14E-15 8.00E-14 -----.. -- 1.25E-12 1.43E-15 8.ooE-14 IEFC 2.00E-l: 2.00E-12 .OOE-12 .OOE-12 .00E-12 2.00E-12 2.00E- .uOE-12 .00E-12 .00E-12 2.00E-12 2.00E-12 2.00H2 ·.OOE-12 2.00E-12 2.00E-12 2.00E-12 2.00E-12 2.00E-12 2.00E-12 2.00E·12 2.00E-12 2.00E-: 1.00E·12 2.00E-12 2.00E-12 Il.OOE-12 2.00E-12 2.00E-12 2.00E-12 2.00E-12 2.00E-12 2.00E-12 2.00E- ~IBHV-5R IO/ml . Pre : Pre: IEFCA Cone 5.ooE-13 1.69E-14 5.00E-13 1.53E-14 5.ooE-13 2.98E-14 5.00E·13 1.80E-15 5.00E-13 2.35E-14 5.00E-13 4.32E-14 15.00E-13 3.01E-14 5.0' 1.83E-14 15.00E-13 14.67E-14 S:OOE-13lz~i1E~14 1.57E-14 2.42E-14 5.00E-13 1.25E-14 5.00£-13 2.15E-14 E~i319~20E=15 5.00E·13 1.13E-16 5.00E-13 2.22E-14 5.00E-13 2.16E-14 5.00E-13 2.02E-14 5.00E-13 2.82E-14 5.00" --, .. -.L::I 1.29E-14 !l.uOE-13 3.28E·14 5.ooE-13 2.77E-14 5.00E-13 1.77E-14 5.00E-13 3.36E-14 5.00E-13 ~14 2.45E- 5.00E-13 3.43E-14 5.00E-13 5.02E-14 5.00E-13 1.43E-14 5.00E·13 1.50E-14 4.09E-: .. 00E-13 3.88E-14 ·.OOE-13 3.49E-14 ·.ooE-13 1.27E-14 5.00E-13 1.56E-14 ,-14 n limit = 6E-13 uCi/ml IBHV-5pa 1.5E-13 uCi/m' 4£-12 uCi/ml 1E-12 uCi/ml EFC ]EFC A 4.00E-12 1.( OE- 4.ooE-12 1.00t.-u 4.00E-12 1.00E-12 4.00E-12 1.00E-12 4.00E-12 1.00E-12 4.00E-12 1.00E-12 4.00E-12 1.00E-12 • OOE-12 1.ooE-12 4.00E-12 11.00E·1 4.00E-12 1t.00E-l: 4.00E-12 4.00E-12 4.00E-12 4.00E-12 4.00E-12 4.00E-12 4.00E-12 4.ooE-12 4.ooE-1: 4.00E-1: 4.00E-12 4.00E-12 4.00E-12 4.00E·l: 4.00E-1: 4.00E-12 4.00E-12 4.00E-12 4.00E-12 4.00E- .00E-12 .00E-12 .00E-12 .OOE-12 1.00E-12 1.00E-12 1.00E- 1.00E-1: .00E-12 .00E-12 1.00E-12 1.00E-12 1.00E·12 1.ooE-12 .00E-12 .00E-12 .OOE-12 1.00E-12 1.00E-12 .00t-li 1.00E-12 1.00E-12 1.00E-12 1.00E-12 1.00E-12 1.00E-12 1.00E-12 1.00E-12 1.25E-12 4.20E-16 8.ooE-14 12.00E-1411.37£-16 12.00E-12 15.ooE-131 1.27E-14 1.25E-12 1.18E-16 8.00E-14 12.00E-14 4.08E-17 12.00E-12 5.ooE-13 3.69E-14 14.ooE-12 11.00E-1 1.25E-12 9.58E-16 8.ooE-14 2.00E-14 8.3lE-17 2.00E-12 5.00E-13 1.43E-14 4.00E-12 1.00E-12 1.25E-12 3.36E·16 8.ooE·14 2.00E-14 1.65E-16 2.00E-12 5.00E-13 1.59E-14 4.00E-12 11.00E-12 1.25E-12 2.25E-16 8.00E-14 2.00E-14 1.08E-16 2.00E-12 5.00E-13 2.24E-14 4.00E-12 '+1.00E-1. 1.25E-12 9.14E-17 8.00E-14 2.00E-14 6.31E-17 2.00E·12 5.ooE-13 3.41£-14 4.ooE-: 1.25E-12 8.25E-16 8.00~-14 2.ooE-14 1.26E-15 2.00E-12 5.ooE-13 1.83E-14 4.00E-12 1 1.00E.] 1.25E-12 1.90E-16 8.00E-14 2.00E-14 2.10E-16 2.00E-12 5.00E-13 1.70E-14 4.00E·12 1.00E-] E-12 8.00E-17 8.ooE-14 2.00E-14 7.00£-17 2.00E-12 5.ooE·13 2.34E-14 4.ooE-12 1.00E-12 I E-12 1.00E-16 8.ooE-14 2.00E-14 5.18E-16 2.00E-12 5.00E-13 3.64E-14 4.00E-12 1.00E-12 I E-12 9.78E-16 8.00E-14 2.00E-14 1.1OE-15 2.00E-12 5.ooE-13 8.30E-15 4.00E-12 1.00E-1il "'~ 1. lIE-IS 8.00E-14 ..,,,n<=1A An<=<=1<: ..,nn".",> <=",,<=.:> ''''''',<: A ""<= ,''' 1 "n<=.111 1.25E-12 1.59E-15 8.00E-14 2.25E-14 9.50E-16 2.00E-14 2.25E-14 8.56E-16 2.00E-14 ~.25E-1411.67E·15 12.(>OE-14 :-14 .. OOE-15 9.70E-17 ,.OOE-15 3.06E-15 ,.ooE-15 ]3.90E-15 IWE:!}_ 2.25E-13 14.34E-15 1.00E-13 2.25E-1315.60E-15 5.ooE-13 1.50E-13 ~J:e IEfflu.l!!!t Conce~tration Limit ~19E-14 uei/~l. _lBHV-5u I Effluent Concentration limit = 12E-14 uei/mllsHV-ST IEffluent Concentration limit = 19E-13 uCi/ml ISHV-sR IEffluent Concentration Limit = I~E-13 u..flLm!_ISHV-5Ps ALARA Goal = 2.25E-14 uCi/ml ALARA Goal = 5E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml ALARA Goal = 1.SE-13 uCi/ml Pre 1994 MPC limit = 5E-12 uCi/ml Pre 1994 MPC limit = 8E-14 uCi/mJ Pre 1994 MPC limit = 2E-12 uCi/ml Pre 1994 MPC limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml I Cone EFC EFe A Cone EFC EFC A Cone EFC EFC A Cone EFC EFC A I 2.04E-14 ._ _ 9.ooE-14 ~E-14 6.70E-15 2.ooE-14 5.ooE-15 7.65E-15 9.ooE-13 2.25E-13 .:\.,.47E·15 6.ooE-13 1.50E-13 12/5/1996 14.50E-14 19.ooE-14 12.25E-1413.58E-14 12.ooE-14 15.ooE-1512.39E-14 19.ooE-13 12.25E-1317.30E-15 16.ooE-13 11.50E-13 1.76E-15 3.57E-15 9.55E-16 7.54E-15 1.50E-13 8/5/1996 2.37E-15 9.00E-14 2.25E-14 8.18E-15 7.46E-16 5.75E-15 1.50E-13 9.39E-16 1.21E-14 1.50E-13 1.84E-16 1.87E-16 9.00E-13 2.25E-13 6.14E-15 1.50E-13 15/5/1997 15.75E-16 6.07E-16 4.75E-15 1.50E-13 U1E-15 5.05E-16 4.92E-15 1.50E-13 1/5/1998 4/28/1998 7/31/1998 8.51E-15 3.75E-15 7/3/1999 1.53E-15 9/27/1999 5.83E-15 "nR/1QQQ 9.48E-15 2.06E-15 1.50j:- [9/26/2000 1.04"- 12/26/2000 1. -.--/2001 4.2j 2001 4.52E-16 /2001 4.65E-16 12/31/2001 4/1/2002 7/1/2002 E-14 12.25E-14 h .92E-15 2.ooE-14 5.ooE-15 6.21E-16 9.ooE-13 2.25E-13 4.68E-15 6.ooE-13 1.50E-13 .38E-15 2.ooE-14 5.00E-15 1.72E-15 9.ooE-13 2.25E-13 7.35E-15 6.ooE-13 1.50E-13 .49E-15 2.ooE-14 5.00E-15 8.34E-16 9.ooE-13 2.25E-13 7.01E-15 6.ooE-13 1.50E-13 E-14 1 2.25E-14"19.20E-16 2.ooE-14 5.00E-15 6.32E-16 9.ooE-13 2.25E-13 3..:~5E-15 6.ooE-13 1.50E-13 9.ooE-14 2.25E-14 4.58E-15 2.ooE-14 5.ooE-15 4.58E-15 9.ooE-13 2.25E-13 1.43E-14 6.ooE-13 1.50E-13 9.ooE-14 2.25E-14 2.45E-15 2.ooE-14 5.ooE-15 2.39E-15 9.ooE-13 2.25E-13 8.46E-15 6.ooE-13 1.50E-13 9.ooE-14 2.25E-14 8.65E-16 2.ooE-14 5.ooE-15 6.52E-16 9.ooE-13 2.25E-13 7.20E-15 6.ooE-13 1.5OE-13 9.ooE-14 2.25E-14 3.52E-15 2.ooE·14 5.00E-15 2.55E-15 9.ooE-13 2.25E-13 8.22E-15 6.00E-13 1.5OE-13 9.00E-14 2.25E-14 6.20E-15 2.00E-14 5.00E-15 3.96E-15 9.ooE-13 2.25E-13 7.56E-15 6.00E-13 1.5OE-13 9.00E-14 2.25E-14 1.27E·15 2.00E-14 5.ooE-15 1.09E-15 9.ooE-13 2.25E-13 7.72E-15 6.00E-l;!. IE-14 2.25E-14 1.24E-15 2.00E-14 5.ooE-15 1.01E-15 9.ooE-13 2.25E-13 4.36E-15 6.00E- 5.45E-16 2.00E-14 5.00E-15 6.01E-16 9.00E-13 2.25E-13 7.67E------- .001;-14 l.l~I;-14 I.~bt-lb L.ool;-14 !l.UOI;-I~ b.84!:-16 9.ooE-13 2.25E-13 7.ooE-15 6.ooE-13 1.50E-l OE-14 2.25E-14 2.19E-16 2.ooE-14 5.00E-15 1.89E-16 9.ooE-13 2.25E-13 6.13E-15 6.ooE-13 1.50E-13 9.ooE-14 2.25E-14 4.02E-16 2.ooE-14 5.ooE-15 1.ooE-16 9.ooE-13 2.25E-13 7.48E·15 6.ooE-13 1.50E·13 9.ooE-14 2.25E-14 2.06E-16 2.ooE-14 5.00E-15 2.02E-16 9.ooE-13 2.25E-13 6.98E-15 6.ooE-13 1.50E·13 ~14 2.25E-14 3.51E-16 2.ooE-14 5.00E-15 3.64E-16 9.00E-13 2.25E-13 4.72E-15 6.00E-13 1.50E-13 .25E-14 7.53E-16 2.ooE-14 5.00E-15 7.19E-16 9.00E-13 2.25E-13 9.65E-15 6.00E-13 1.50E-13 3.39E-16 9.00E-13 2.25E-13 7.20E-15 6.ooE-13 1.50E-13 E-14 1 2.25E-14"19.28E-16 2.ooE-14 5.00E-15 3.14E-16 9.00E-13 2.25E-13 4.48E-15 6.ooE-13 1.50E-13 1.00E-16 19.00E-14 2.25E-1417.67E-16 2.ooE-14 5.00E-15 3.48E-16 9.ooE-13 2.25E-13 9.56E-15 6.ooE-13 1.50E-13 1.:.13E-15 9.ooE-14 2.25E-1417.41E-16 2.00E-14 5.00E-15 4.41E-16 9.ooE-13 2.25E-13 6.68E-15 6.00E-13 1.50E-13 4.35E-16 9.ooE·14 2.25E-14 5.mU 'E-16 2.ooE-14 5.ooE-15 2.51E-16 9.ooE-13 2.25E-13 1.34E-15 6.ooE·13 1.50E-13 1.51E-16 9.ooE-14 2.25E-14 1.02E-16 2.ooE-14 5.ooE-15 1~ ,09E-16 9.00E-13 2.25E-13 7.28E-15 6.ooE-13 1.50E-13 ---~ ------------------------------11.52E-16 9.ooE-14 2.25E-14 1.54E-16 2.ooE-14 5.ooE-15 1.5u-.1!;! ::MIU!:-.1;) ':.'::>~-.1:> I.V':!:-.1;) !;!.VlJt-.1';) .1.:>Vt-.1';) 1/29/2004 11.ooE-16 9.ooE-14 2.25E-14 1.12E-16 2.ooE-14 5.ooE-15 l.ooE-16 9.ooE-13 2.25E-13 8.82E-15 6.ooE-13 1.50E-13 .18E-16 9.ooE-14 2.25E-14 3.11E-16 2.ooE-14 5.00E-15 1.25E-16 9.ooE-13 2.25E-13 2.47E-15 6.ooE-13 1.50E-13 1.16E·16 9.00E-14 2.25E-14 1.72E-16 2.ooE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 1.10E-14 6.ooE-13 1.50E-13 7/2004 1.14E-16 9.00E-14 2.25E-14 1.06E·16 2.ooE-14 5.ooE-15 1.00E-16 9.00E-13 2.25E-13 1.59E-14 6.00E-13 1.50E-13 /2005 l.ooE-16 ----. . ----. -- 7/3/2006 3.08E-16 9.ooE-14 2.25E-14 1.10E-16 2.ooE-14 5.ooE-15 1.00E-16 [9.ooE-13 [2.25E-l 10/2/2006 9.14E-16 9.ooE-14 2.25E-14 4.95E-16 2.ooE-14 5.ooE-15 1.8"" 11:: n nM • ., .J? .,~ .... 1/1/2007 9.49E-16 9.ooE-14 2.25E-14 6.81E-16 2.ooE-14 5.ooE-15 2.02E-16 9.00E-13 ...ll-.25E-13 1.31E-14 .J§.ooE-13 ...11.50E-13 4/2/2007 1.08E-15 9.ooE-14 2.25E-14 8.22E-16 . __ LOOE~14 5.ooE-15 2.26E-16 .19.OOE-13 ...E.25E-lll1.64E-14 .J.6.ooE-13 ...11.50E-13 !/2oo7 [1.54E-15 [9.ooE-14 [2.25E-1418.16E-16 12.ooE-14 [5.ooE-15 4.76E-16 9.ooE-13 2.25E-13 2.12E-14 6.00E-1';) 1.::'Ut-l.;) ~.90E-16 -¥.'.OOE-14 ...g.25E-l":-f.37E-16 ...g.OOE-14 5.00E-15 l .ooE-16 9.00E-13 2.25E-13 6.65E-15 6.ooE-13 1.50E-13 DE-IS 1.00E-16 9.ooE-13 2.25E-13 1.02E-14 6.00E-13 1.50E-13 1.46E-15 9.00E-14 2.25E-14 5.67E-16 12.00E-14 15.(' 1/2008 3.16E-16 9.00E-14 2.25E-14 6.17E-16 2.00E 14 5.ooE-15 3.71E-16 9.00E-13 2.25E-13 4.82E-15 6.ooE-13 1.50E-13 0/2008 3.13E-15 9.00E-14 2.25E-14 1.55E-15 2.00E-14 5.00"· .. ,, ".~H -.----9.00E-14 2.25E-14 2.00E-14 5.ooE-15 19.ooE-13 12.25E-131 ~.ooE-13 t.50E-13 4.13E-15 2.31E-16 3.10E-15 LooE-14 2.25E-14 2.00E-14 5.00E-15 9.ooE-13 12.25E-13 16.ooE-13 1.50E-13 19.ooE-14 2.25E-14 1.39E-15 2.ooE-14 5.ooE-15 1.41E-15 J.9.00E·13 J3.25E-13~.66E-15 .l?ooE-13 J.t.50E-13 7.79E-16 6.37E-16 4.18E-15 1.50E-13 9.ooE-14 2.25E-14 9.20E-16 2.ooE-14 5.00E-15 6.36E-16 9.ooE-13 2.25E-13 1.21E-14 6.ooE-13 1.50E-13 9.ooE-14 2.25E-14 3.13E-16 2.ooE-14 5.00E-15 1.92E-16 9.00E-13 2.25E-13 2.48E-15 6.00E-13 1.50E-13 Date Effluent Concentration Limit = 9E-14 uCi/mi BHY-SU Effluent Concentration limit = 2E-14 uCi/ml BHY-5f Effluent Concentration limit = 9E-13 uCi/ml BHY·SR Effluent Concentration limit = 6E·13 uCi/ml BHV-SPB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal :: SE-13 uCi/ml ALARA Goal = 2.2SE-13 ud/ml ALARAGoal = l.5E-13 uCi/ml Pre 1994 MPC Limit = 5E-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit:: 2E-12 uCi/mi Pre 1994 MPC Limit = 4E-12 uCi/mi Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/m[ Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFC A 3/31/2010 4.78E·15 9.00£·14 2.2SE·14 3.73E·16 2.ooE·14 5.00E·15 4.19E·16 9.00E·13 2.25E·13 1.30E·14 6.ooE·13 1.50E·13 6/30/2010 4.35E·15 9.ooE·14 2.25E·14 7.84E·16 2.ooE·14 5.ooE·15 1.05E·15 9.00E·13 2.25E·13 4.40E·15 6.ooE·13 1.50E·13 9/30/2010 3.57£·15 9.00£-14 2.25£·14 1.14£-15 2.00£-14 5.00£·15 7.97£·16 9.00£·13 2.25E-13 3.78E·15 6.ooE·13 1.50£·13 12/31/2010 8.52£-15 9.00£-14 2.25£-14 1.45E-15 2.00£-14 5.ooE-15 1.29E-15 9.00£-13 2.25£-13 1.33E-14 6.ooE-13 1.50E-13 If) I: o :;:; ~ .. I: CD U I: o U CD :2 U :::I I: .2 '0 ~ It) ::> :J: In N '" ~ ~ , , w w 0 0 C> C> ~ ~ ,. .. ~ < "If ~~ 1.[:;' t!. ~l¥P I ,~! I. ~ >«. ~ ~ .~ "' .... It ~,..t , -, ... ~ , w 0 C> ~ ~ l-+ ~ I .~ .;. ~ II ~ 9 --;;t ~ I ~ I I -~ ~R'" '" ~ , w 0 C> ~ (aleos 501) o~-das 60-das so-das ~ Lo-das 90-das :::::; ~I 90-das c ~ vo-das ~ ,;::;~ £O-daS 0 ~ lO-daS N , "0 .. ~o-das '" .3 oo-das + 66-das C!) N N S6-das , E :::J L6-das '0 '" 0:: 96-das + 96-daS 0 '" v6-daS N , E :::J £6-daS 'C 0 .r::; r.< l6-daS r- + ~6-das 06-das Oi ~ .3 '" 6s-das z E SS-daS :::J 'c '" ~ LS-daS ::::> + 9S-daS gs-das vS-daS £S-daS lS-daS ~s-das C!) "-co ~ ~ ~ , , , w w w 0 0 0 C> C> 0 ~ ~ 1.00E-11 1.00E-12 1.00E-13 ID ~ en1.00E-14 Cl o 2- 1.00E-15 1.00E-16 1.00E-17 i~ ~ (X) 6. 0) en Effluent Concentration Limit = 9E-14 uCilml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml M'r. ~ r ! \j*1 \ \. I~ N M .... '" "' r--(X) Cl 0 (X) (X) (X) (X) (X) (X) (X) (X) Cl 6. 6. , 6. 6. 6. 6. 6. 6. 0. 0) 0) 0) 0) 0) 0) 0) 0) 0) en en en en en en en en en ~ Cl 6. 0) en BHV-5 Uranium-Natural Concentrations (uCi/ml) , --~-~ I~ ~ \ tJ ~~ ,.,. .j, -=,.= - :-}-M - ~---- T ~ N M .... '" "' r--(X) Cl 0 ~ N M .... '" "' r--(X) Cl 0 Cl Cl Cl Cl Cl Cl Cl Cl 0 0 0 0 0 0 0 0 0 0 ~ 6. 6. 6. 6. 6. , , , , , , , , , , 6. 6. 6. 6. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) en en en en en en en en en en en en en en en en en en en Vl C o ~ ... C CP U C o U o M ('oj • E ::::I ';: o .c I- In :> ::I: m I I N C') ~ ~ , , UJ UJ 0 0 0 ~ ~ ~ I .. .. C t:.. I ;; I I t... .... ~ , UJ 0 ~ (aleos 601) .... o ~-das 60-das .... I .. go-das -I Lo-das 90-das go-das -. P. .:::: ~ vo-das £O-daS GQ-daS ;: ~o-das -t' oo-das P 66-das ~ g6-das ~ L6-das 96-daS 96-daS I ~ v6-daS £6-daS .... p (:6-daS ~6-das 06-das I 6g-das gg-daS L9-daS 99-daS gg-das "";:: vg-das .--4 £g-daS c::g-daS ~g-das '" <!} ..... ~ ~ ~ , , , UJ UJ UJ 0 0 0 ~ ~ ~ ~ ~ If) c:: o .. E ... c:: Q) C) c:: o U 10 N N • E :::I " ." D:: It) :> J: III ~ ~ , W 0 C> ~ ~ ... N ~ , W 0 C> ~ ... ~ • 5 I~ 0') ..- ~ ~ , , W W 0 0 C> C> ~ (ale~s 601) ... N f+" r-.. ~ I..:: • • ~ on ~ , W 0 C> ~ ~ ~ .;: V ~I I <D ~ , W 0 C> ~ - - I "-~ , W 0 C> ~ o~-das 60-das BO-daS Lo-das 90-das 90-das vO-daS £O-daS lO-daS ~o-das oo-das 66-das B6-das L6-das 96-daS 96-daS v6-daS £6-daS l6-das ~6-das 06-daS 6B-daS BB-daS LB-das 9B-das 9B-daS vB-das £B-das lB-das ~B-das I/) c: o ~ .... c: II) o c: o u o .... N • "C ell ~ It) :> J: In ~ ~ , W 0 0 ~ N '" ~ ~ , , W W 0 0 c:> c:> ~ ~ o~-das 60-das I go-das ~ LO-daS 90-daS 9O-daS ~ vO-daS £O-daS lo-das I I ~o-das OO-daS 66-daS ..::: 96-daS , L6-daS • 96-das g6-das v6-das ~It , ..... :!. £6-das l6-das "--;::- N ~6-das I~ 06-daS ::1 69-daS ) gg-das f • '..., Lg-das 99-daS • ~ A gg-das vg-das (' £g-das 19-das .., ~g-das ... lO CD r-- ~ ~ ~ ~ , , W W , , W W 0 0 c:> c:> 0 0 c:> c:> (alB:>§" 501) ~ ~ ~ TAB 6 BHV-6 AIR SAMPLING GRAPHS AND DATA TABLE loate 10/1982 ~7/1982 1/1983 1/1983 14/2/1984 17/2/1984 ./2/1986 4/1/1986 6/30/1986 1O/27/198E 9/9/1987 11/2/1987 '!/16/1988 /14/1990 /13/1990 1fn/1QQ( 11/1991 0/1992 1/1992 !2/9/1993 0/1993 '8/1993 /1994 IEffluent Concentration limit = 19E-14 uCi/ml IBHV-6U I limit = 12E-14 uCi/mI IBHV-6T 1 Effluent Concentration Limit = 19E-13 uCi/ml IBHV-6R IEffl uent Concentration limit = 16E-13 uCi/ml 18HV-6PB ALARA Goal = ALARA Goal = 15E-13 uCi/ml l ALARA Goal = ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC limit = Pre 1994 MPC limit = Pre 1994 MPC Limit = Pre 1994 MPC limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = lE-12 uC/lml EFC 5.00E-12 1.25E-12 8.00E-14 l2.ooE-14 12.00E-12 15.00e-l 4.ooE-12 l.OOE-12 5.00E-12 1.25E-12 8.00E-14 8.00E-14 8.00E-14 8.00E-14 8.00E-14 2.ooE-14 2.ooE-14 2.00E-14 2.ooE-14 2.ooE-14 12.ooE-12 5.00E-13 4.ooE-l 4.00E-l 4.00E-12 4.00E-12 l.ooE-12 5.00E-12 1.25E-12 2.00E-12 5.00E-l ~ 5.00E-12 1.25E-12 2.00E-12 5.00E-l 1.00E-12 5.ooE-2.00E-12 5.ooE-13 2.00E-12 5.00E-13 OE-12 s:oci'E-12 11.25E-12 ~ ;1.ooE-12 5.00E-12 5.00E-12 5.00E-12 1.25E-l" 1.25E-l' 1.25E-l' 8.00E-14 8.00E-14 8.00E-14 2.00E-12 5.00E-l 2.00E-12 5.00E-l 2.ooE-12 5.00E-l 2.ooE-12 5.00E-13 4.ooE-l;; 4.00E-l;; 4.00E- l.ooE-12 ~ ~ 11.ooE-12 5.00E-12 11.25E-12 LooE-14 2.ooE-14 2.ooE-12 5.ooE-13 ~.ooE-12 ~.OOE-l' i1.00E-12 5.00£-12 1.25E-l; LooE-14 8.ooE-14 8.00E-14 2.ooE-14 2.ooE-14 2.ooE-l' 2.ooE-12 5.ooE-13 kOOE-l; 11.ooE-12 5.ooE-12 1.25E·l; 2.00E-12 5.00E-13 5.ooE·12 1.25E·l; 2.ooE-12 5.00E-13 5.ooE·12 5.00E-12 5.00E-12 )oE-l .00E-l )OE-l )oE-l: 5.ooE-12 5.00E-l 5.ooE-l 5.00E- •. OOE-12 ;.OOE-12 5.ooE-l; OE-l ' .OOE- (lE-12 ;.ooE-I' ;.OOE·l; 5.ooE-l; ~ -;.OOE-12 ;.ooE-12 i.ooE-l; 5.ooE-l; DE-I: DE-12 .ooE-12 DE-I: 1.25E-12 l.ooE-1 1.25E·12 1.ooE-12 1.25E-12 l.ooE- 1.25E-12 8.ooE-14 2.ooE-14 2.ooE-12 5.ooE-13 4.ooE-12 1.ooE- 1.25E-12 8.ooE·14 2.ooE-14 2.ooE-12 5.ooE·13 4.ooE-12 1.ooE- 1.25E-12 8.ooE-14 2.ooE-14 2.ooE-12 5.ooE·13 4.ooE-12 1.001 1.25E-12 8.ooE-14 2.00E-14 2.00E-12 5.ooE-13 _ 4.00E-12 l.ooE-12 1.25E-12 8.ooE-14 2.ooE-14 2.ooE-12 5.ooE-13 4.00E-12 1.ooE-12 1.25E-12 8.00E·14 2.00E-14 2.ooE-12 5.ooE-13 4.ooE-12 1.ooE-12 1.25E-12 8.00E-14 2.ooE-14 2.ooE-12 5.00E-13 4.00E-12 1.00E-12 1.25E-12 8.00E-14 2.ooE-14 2.ooE-12 5.00E-13 4.00E-12 l.ooE-12 l.l5t-U l.ooE-12 1.25E-12 l.ooE-12 1.25E-12 l.ooE-12 1.25E-12 8.ooE-14 2.ooE-14 2.00E-12 5.Wt-lj 4.l 0'· 1.25£-12 8.00£-14 2.ooE-14 2.ooE-12 5.ooE-13 4.ooE-U l.(JOE-12 1 1.25E·12 8.ooE-14 2.ooE-14 2.ooE-12 5.ooE-13 4.ooE-12 1.00E-12 1.25E-12 8.ooE-14 2.ooE-14 2.ooE-12 5.ooE-13 4.00E-12 l .ooE-12 1.25E-12 8.ooE-14 2.ooE-14 2.ooE-12 5.ooE-13 4.ooE-12 1.00E-12 1.25E·12 8.ooE-14 2.00E-14 2.ooE-12 5.ooE-13 4.00E·12 1.00E-12 1.25E-12 8.ooE-14 2.00E-14 2.00E-12 5.ooE-13 4.ooE-12 1.ooE-12 1.25E-12 8.ooE-14 2.ooE-14 2.ooE-12 5.ooE-13 4.ooE-12 1.ooE-12 1.25E-12 8.ooE-14 2.ooE-14 2.ooE-12 5.ooE-13 4.ooE-12 l.ooE-12 1.25E-12 8.ooE-14 2.ooE-14 2.ooE-12 5.ooE-13 14.ooE-12 11.00E-12 1.25E-12 8.00E-14 2.ooE-14 2.ooE-12 5.ooE-13 1.25E-12 8.ooE-14 2.ooE-14 2.ooE-12 5.ooE-13 1.25E-12 8.00E·14 2.ooE-14 2.00E-12 5.ooE- 1.25E-12 8.ooE-14 2.ooE-14 2.ooE-12 5.ooE-l 1.25E-12 8.ooE-14 2.ooE-14 2.ooE-12 5.ooE-13 1.25E-12 8.ooE-14 2.ooE-14 2.ooE-12 [5.ooE-l 1.25E-12 8.ooE-14 2.ooE-14 2.ooE-12 -#.ooE-1 L.25E-12 8.ooE-14 2.ooE-14 2.ooE-l; 25E-12 8.ooE-14 2.ooE-14 2.00E-~ .25£·12 8.00£-14 2.00E· 2.00£-12 2.ooE-l; OE-1 14.00~1~_ 4.ooE-12 4.00£-12 OE-l 1 .. oo~:!l. l.ooE-12 1.00£·12 '/1994 2.00£-1; 5.ooE-~ 5.ooE-: OE-: 14.ooE-12 4.ooE-12 OE-! 1.00£-12 1.00E-12 '1994 8.00E-14 12.ooE-141 12.ooE-12 8.00E-14 2.OOE-14 5.' 5/9/1995 9.ooE-14 2.25E-14 2.00£-14 5. 8/9/1995 9.00E-14 2.25E-14 2.00E-14 5 .. 5.ooE-l: 4.00E-12 1.00E-l [Date ~I 51 81 i!1996 i!1996 7/31/1998 9/28/1998 12/28/199E 17/3/1999 [ALARA Goal = [Pre 1994 MPC limit = 13.03E-15 12/28/1999 5.01E-15 3/30/2000 7.46E- 5.40E-16 26/2001 2/2001 3.75E-16 5.21E-16 42E-16 ;-16 31E-16 /1/2002 4.77E-16 17/1/2002 3.68E-16 9/30/2002 [3.67E-16 12/30/2002 3/31/2003 1.98E-16 '/~O/Z003 3/29/2004 1.00E-16 6/27/2004 1.00E- 1.00E-16 1.05E-16 1.00E-16 1/2006 1/2oo&. l/2oo7 1/2/2007 ~ 3.25E-16 5.03E-16 8.31E-16 7/2/2007 Il.U><'" 9/30/2007 12/31/200712.9 ~f":l:1 "MA 14.34E-16 1.88E-15 /31/2008 15/2009 IU-mit;' 19E-=14- 4 uCi/ml al :: [5E-12 uCi/ml [Pre 1994 MPC limit = 1.25E-12 uCi/ml IEFC IEFCA Icone 2.25E-14 9.00E-14 2.:t~t·14 9.00E-14 l-,-25E .• 14_ 9.00E-14 2.25E-14 9.ooE-14 2.25E-14 9.ooE-14 ---f2,"25E:14 9.00f 9.00E-14 12.25E-14 9.00E·14 2.25E·14 9.00E-14 2.25E-14 9.ooE-14 [2.25E-14 2.25E- 9.ooE-14 2.ht-14 9.00E-14 2.25E-14 9.00E-14 2.25E-14 9.00E-14 2.25E-14 1.37E-15 9.00E-14 2.25E-14 2.89E-15 2.25E-14 5.25E-16 9.00E-14 9.00E-14 9.00E-14 9.00E-14 I.00E-14 I.00E-14 9.00E-14 9.00E-14 9.00E-14 9.00E- I.ooE-14 l.ooE-14 l.ooE-14 l.ooE-14 E-14 .ooE·14 I.OOE-14 I.00E-14 9.ooE-14 9.00E-14 9.ooE· 9.ooE-14 l.ooE-14 ~ 2.:QQE-14 9.00 E-14 9.00E-14 9.00E-14 E-14 E-14 E-14 :-14 2.25E-14 3.53E-16 2.25E-14 [2.23E-16 25E-14 .25E-14 .25E-14 2sE-i4"11.01E-: 2.25E-14 1.25E-16 2.25E-14 2.94E-16 .25E-14 .25E-14 .25E- .l5E-14 2.25E-14 1.15E-16 2.25E-14 1.00E-16 2.25E-1411.36E-16 1.00E- 2.25f.l4 1.00E-16 2.25E-14 1.38E-16 2.25E-14 1.72E-16 2.25E-14 1.00E-16 !.25E-14 1.01E-16 1.25E-14 5.98E-16 2.25E-14 2.88E-16 2.25E-14 2.ooE-16 2.25E-14 2.36E-16 !.25E-14 1.49E-ll 25E-14 1.55E-15 2.25E-14 3.51E-16 1.25E-14 9.00E-16 !.25E-14 2.25E-14 2.25E-14 1.01E-15 2.25E-14 2.67E-16 4.32E-16 2.26E-16 IALARA Goal :: I Pre 1994 MPC limit :: [EFC 2.00E-14 2.00E-14 2.00E-14 ()E-14 .OOE- [EFC A [Cone 5.ooE-15 5.ooE-15 5.00E-15 IE-IS ()E-14 [5.00E-15 !.OOE-14 5.ooE-l! 2.ooE-14 5.00E-l! 2.00E-14 5.00E-l! 2.ooE-14 5.00E- ~.UUt-14 5.00E-l! !.ooE-14 5.00E-l! !.ooE-14 5.00E-l: 2.00E-14 5.00E-15 8.72E-16 2.00E·14 5.00E-15 1.31E- ~.OOE-14 5.00E-15 3.00E-16 !.ooE-14 5.00E-15 6.11E-16 !.ooE-14 5.00E-15 1.91E-16 2.ooE-14 5.00E-15 3.28E-17 2.00E-14 5.ooE-15 1.00E- 2.00E-14 5.00E-15 1.00E-16 !.ooE-14 5.ooE-15 1.77E-16 2.00E-14 5.00E-15 1.09E-16 2.00E-14 5.00E-15 1.96E-16 2.00E-14 5.00E-15 1.76E-16 2.00E-14 5.ooE-15 1.80E- 2.00E .~ -----,~.wt-.d 1.67E-16 1.00E-14 15.ooE-15 1:00E-16 2.00E-14 2.00E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 2.00E-14 5.ooE-15 l.ooE- 2.00E-14 5.ooE-15 1.00E-16 2.ooE-14 5.00E-15 1.00E-16 2.00E-14 5.00E-15 1.00E·16 2.ooE-14 5.00E-15 1.00E·16 2.ooE-14 5.ooE-15 1.00E-16 2.ooE-14 5.ooE-15 3.55E-16 2.ooE-14 5.ooE-15 3.60E-15 2.ooE-14 5.ooE-15 1.00E-16 :-14 2.00E-14 2.00E-14 :-14 E-14 12.ooE-14 .. , '.Wt-l~ 1.54t-10 ;.OOE-15 1.00E-16 i.OOE-15 3.16E-16 ;.OOE-15 1.00E-16 4.04E-16 7.82E-16 i.OOE-151.!&1E-16 2.23E-16 1.15E-16 AGOAl:: 2.25E-13 uCi/ml 2E-12 uCi/ml 5E-13 uCi/ml EFe 9.ooE-13 9.ooE-13 9.00E-13 9.00E-13 9.00E- ~.OOE-13 ~.OOE-13 9.ooE-13 1.00E-13 1.00E-13 '.OOE-13 ooE-13 9.00E-13 9.00E-13 9.00E-13 9.00E-13 9.00E-13 9.00E-13 9.ooE-13 9.ooE-13 9.00E-13 9.ooE-13 9.00E-13 9.00E-13 IE-13 OE-13 9.00E-13 9.00E-13 9.ooE-13 9.00E-13 9.00E-13 9.ooE-13 9.00E-13 9.00E-13 9.00E-13 l.ooE-13 l.ooE-13 9.00E-13 1.00E-13 1.00E-13 1.00E-13 1.00E-13 9.00E-13 9.00E- 1.00E-13 I.00E-13 I.00E-13 2.25E-13 2.25E-13 2.25E-13 2.25E-13 2.25E-13 ~J5E-13 2.25E-13 2.25E-13 2.25E- 2.25E·13 2.25E-13 2.25E-13 25E- .25E- E-15 25E-13 7.83E-15 2.25E-13 4.83E-15 2.25E-13 6.41E-15 2.25E-13 8.57E-15 2.25E- 2.'i"SE-1316.95E-15 2.25E-13 8.59E-15 2.25E-13 3.14E·15 .25E-13 8.6lE-15 .25E-13 8.20E-15 ......... -.. " ,:>.:>:>e-15 25E-13 1.35E-14 2.25E-13 7.77E-15 2.25E- 2.25E-1 2.25E-1 l.loSE-l 2.25E·13 3.55E-15 2.25E·13 1.22E-14 2.25E-13 1.52E-14 2.25E- l.l5E-13 9.85E-15 2.25E-13 1.71E-14 2.25E-13 4.85E-14 2.25E·13 1.11E-14 ,J!10E-14 ~ E-14 2.25E-13 2.04E-14 2.25E·13 6.38E-15 2.25E-13 9.19E-15 2.25E-13 5.99E-15 2.25E-13 7.41E-15 2.25E- .l~E-] 25E-13 6.46E-15 2.25E-13 5.76E-15 8.98E-15 6.44E-15 al :: [EFC EFCA ;.OOE-13 1.50E-13 ;.OOE-13 1.50E-13 ;.OOE-13 1.50E·13 6.00E-13 11.50E-13 6.00E- -:;:ooE.13 11.50E-13 ;.OOE-13 1.50E-13 ;.OOE-13 1.50E-13 ;.OOE-13 [1.50E-13 6.ooE·13 1.50E-13 6.ooE·13 1.50E-13 ;.ooE-13 1.50E-13 ;.ooE-13 1.50E-13 6.ooE-13 1.50E-13 6.00E-13 1.50E-13 6.ooE-13 1.5OE-13 6.00E-13 1.5OE-13 6.00E-13 1.5OE-13 6.00E-13 1.50E-13 6.ooE-13 1.50E-13 6.ooE-13 1.50E-13 6.00E-13 1.50E-13 6.00E-13 1.50E-13 16.00'." 1'·50E." ,.OOE- .OOE- 1.50E- 1.5nF- OE-13 11.50E-: 1.50E-13 1.50E·13 1.50E-13 6.00E-13 1.50E-13 6.00E-13 1.50E-13 6.00E-13 1.50£-13 6.00E-13 1.50E-13 6.00E-13 1.50E-13 6.00E·13 1.50E-13 6.00E·13 1.50E-13 6.00E-13 6.00E-13 6.00E-13 6.00E-13 6.00E-13 6.00E-13 6.00E-13 6.00E-13 1.50£-13 1.50E-13 1.50E-13 1.5OE-13 1.5OE-13 1.5OE-13 1.50E-13 '·1 '·1 1.50£-13 1.50E-13 1.50E-13 1.50E-13 Date Effluent Concentration limit = 9E-14 uCi/ml BHV-6U Effluent Concentration Limit = 2E-14 uCi/ml BHV-6T Effluent Concentration limit = 9E-13 uCi/ml BHV-6R Effluent Concentration Limit = 6E-13 uCi/ml BHV-6PB ALARAGoal = 2.25E-14 uCi/ml ALARAGoal = 5E·13 uCi/ml ALARAGoal= 2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 5E-12 uCi/ml Pre 1994 MPC Limit = BE-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL-5E-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFC A Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 3/31/2010 9.63E·1S 9.00E-14 2.2SE-t4 1.82E·t6 2.00E-14 S.OOE-IS 2.06E-16 9.00E-13 2.25E·13 1.37E-14 6.00E-13 1.SOE-13 6/30/2010 3.62E-15 9.00E-14 2.2SE-14 3.94E-16 2.00E-14 S.OOE-IS 4.89E-16 9.00E-13 2.2SE-13 4.30E-IS 6.00E-13 1.SOE-13 9/30/2010 S.42E-1S 9.00E-14 2.25E-14 1.OSE-1S 2.00E-14 S.OOE-1S S.68E-16 9.00E-13 2.2SE-13 3.98E-1S 6.00E-13 1.S0E-13 12/31/2010 1.24E-14 9.00E-14 2.2SE-t4 t.2lE-lS 2.00E-14 S.OOE·1S 1.00E·1S 9.00E-13 2.2SE·13 1.S3E-14 6.00E-13 1.S0E-13 f/) c o ~ ... c CI) o c o U CI) :E "0 :I C o "C III 0:: U) ::> J: m N ~ , w ~ I ~ ... I 1St 4 ..l i+--- ~ ..: I ... .A ~ I '~ --.::::. ~L • ;;'41 ~ f-~ ~ ~ I I 900<:/0£/6 900l19l16 o ~ lOOlIO£/1f6 ~ ---' + 666~/alfW C)I E .;1 & 966~/9/9 + g C)I E :::> £66~/0~/9§ .s:: f- + 066~/£~/~ c;; z E :::> '1" ~ L96~/6/6 + ~96 ~l\lll6 1.00E-11 1.00E-12 1.00E-13 Q) ro () UJ1.00E-14 Cl o ~ 1.00E-15 1.00E-16 1.00E-17 ~ ex> '" ~ -ex> N -'" Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml , , , , '" , , " "" "-0 ex> ex> '" '" '" '" ~ ~ ~ -~ -~ '" -~ 0 -~ ex> " , , , , , '" '" '" ~ -0 ~ -ex> BHV-6 Uranium-Natural Concentrations (uCi/ml) 1 - tf- • "$J.~: : -- ... .. ., t.I I ~ IA J - '" , , , , , , , " , , , , , CD '" N '" ex> '" '" 0 0 0 '" '" 0 0 0 ~ ~ ~ ;a 25 i?5 -"-0 co N '" ~ '" --0; '" '" '" 1.00E-11 1.00E-12 1.00E-13 Q) ~ <n1 .00E-14 Cl ~ 1.00E-15 1.00E-16 1.00E-17 ~ co Ol ~ -co N a; Effluent Concentration Limit = 2E-14 uCi/ml ALARA Goal = 5E-13 uCi/ml Pre 1994 MPC Limit = 8E-14uCi/ml " r--a co co Ol Ol Ol Ol ~ ~ ~ -a; -~ '" 25 a; ~ co '" Ol Ol ~ -a ~ co BHV-6 Thorium-230 Concentrations (uCi/ml) CD Ol Ol ~ ~ ~ J Ol Ol Ol ~ ;::: ~ ¥ r \ IN \AA N a a l3 a5 , , ~ f"6 '" a a ;a ~ ¥ \ '" " a a N 25 '" a; .... I .. 1.00E-11 1.00E-12 1.00E-13 Q) ro u Ul1 .00E-14 Cl 2 1.00E-15 1.00E-16 1.00E-17 ~ <Xl C) ~ co N as Effluent Concentration Limit = 9E-13 uCilml ALARA Goal = 2.25E-13 uCilml Pre 1994 MPC Limit = 2E-12uCilml Pre 1994 ALARA Goal = 5E-13 uCilml , , " , v r--0 <Xl <Xl C) C) C) C) ~ ~ ~ -as ?i ~ a as ~ -<Xl \ (") C) C) ~ a ~ -<Xl BHV-6 Radium-226 Concentrations (uCi/ml) <0 C) C) ~ !!:! <Xl ~ C) C) C) ~ ;::: ~ N\ N o o l3 ill ~J..J '" , , '" LD o o ii5 ~ o o ~ o (") as I. 'y 1.00E-11 1.00E-12 1.00E-13 Q) ~ (l)1.00E-14 Cl o 2- 1.00E-15 1.00E-16 1.00E-17 ~ <X> '" ~ a:; ~ Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994ALARA Goal = 1E-12 uCi/ml ..,. r--<X> <X> '" '" ~ ~ -~ ~ 25 ~ a '" '" ~ -'" ~ a:; '" '" Ol ~ -a ~ a:; BHV-6 Lead-210 Concentrations (uCi/ml) CD '" '" ~ in a:; '" '" '" ~ ;::: ~ , , ~ N a a N 25 '" a; 1\1 co a a ~ N a; .. ~ - - a a ~ a '" a; ~ 1 - ATTACHMENT C AIR PARTICULATE LABORATORY RESULTS AND QAlQC EN:RGY 1 "\ ! "l'!' 1'1 www.energylab.com _--'1$1 He~na, MT 871-412-0711 • Billings, MI 808-135-4419 . Casper, W'/888-235-0515 GIII.H., W'/816-6B8-J1J5 • Rapid CItj, SD 888-&12-1225 • ColI.ge St.tlon, Jl8B8-690-2218 December 06, 2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: Cl0l00417 Project Name: 3rd Quarter BHV Air ANALYTICAL SUMMARY REPORT Energy Laboratories, Inc. received the following 6 samples for Denison Mines USA Corp on 10/8/2010 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test Cl0l00417-001 BHV-l 10/04/10 00:00 10/08/10 Filter Composite of two or more samples Metals, Total Digestion, Total Metals Lead 210 Radium 226 Thorium, Isotopic Cl0l00417-002 BHV-2 10/04/10 00:00 10/08/10 Filter Same As Above Cl0l00417-003 BHV-4 10104/10 00:00 10/08/10 Filter Same As Above Cl0l00417-004 BHV-5 10/04/1000:0010/08/10 Filter Same As Above Cl0l00417-005 BHV-6 10/04/1000:0010/08/10 Filter Same As Above Cl0l00417-006 Blank 10/04/10 00:00 10/08/10 Filter Same As Above This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QNQC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: k~ Technical Director Digitally signed by Steve Carlston Date: 2010.12.06 11 :52:33 -07:00 Page 1 of 23 'II'tNI.energylab.com ___ ,m H,~na, MT 877-412-0111 • Billings, MT 801-135-4489 • Casper, WY 889-235-0515 GIII.tt. WY 81&-&8&-7175 · Ra Id C SD 888-&12-1225 · Coli •• Station IX 888-&90-2218 CLIENT: Projec1: Denison Mines USA Corp 3rd Quarter BHV Air Sample Delivery Group: C 1 01 00417 ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Report Date: 12/06/10 CASE NARRATIVE Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. Page 2 of 23 EN:RGY J\-IC'PI\I '1I1 " WNN.energylab.com AiIM1tIaf ExuIItIJcISkIu 1152 Helena, MT 877·412·0111 • Billings, MT 800·135·4489 • Cesper, WY 888·235·0515 Gillette, WY 866·686·1115 . Rapid City, SD 888·672·1225 . College Station, IX 888·690·2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: December 6, 20)0 PROJECT: 3rd Quarter DHV Air SAMPLE 10: BHY.) QuartcrlDatc Sampled Radionuclide Concentration Air Volume pCUmL C I 0040255·00 I ~'U 1.97E·15 First Quarter 20 I 0 ''''Th 2.15E·t6 Air Volume in rnU "'Ra 3.27E·t6 1.36E+11 210Pb 1.00E·t4 QuartcrlDate Sampled Concentration AirVoJume Radionucllde pCUmL CIOO70338·00 t ~'U 1.5SE·15 Second Quarter 2010 ''''Th 4.7 IE·16 Air Volume in mu. 226Ra 7.70E·16 1.36E+11 2IDPb 4.07E·15 Counting Precision pCUmL N/A 3E·17 9E·t S 9E·17 Counting Precision pCVmL N/A 5E·J7 3E·17 6E·17 QuarterlDatc Sampled Concentration Counting Air Volume Radionuclide pCUmL CtOI00417·00t ~'U 8.42E·16 Third Quaner 2010 ""Th 2.S0E·16 Air Volume in mLs ""Ra 1.31E·16 1.37E+11 2lOPb 6.S0E·15 +LW's are from Reg. Guide 4.14 ·Effluent Concentration from the NEW to CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lcad-210 Precision pCUmL N/A 5E·J7 IE·J7 IE·16 MDC pCUmL N/A 5E·tS 2E·IS 5E·J7 MDCpCUmL N/A 5E·IS 6E·tS 6E·t7 MDCpCVmL N/A 7E·IS 6E·18 7E·17 L.L.D.+ Effluent Cone.· % Emuent pCUmL pCUmL Concentration IE·t6 9E·14 2. I SE+OO tE·t6 3E·1 4 7.17E·01 tE·t6 9E·13 3.63E·02 2E·t5 6E·13 1.67E+OO L.L.D.+ Emuent Cone.· % Emuent pCUmL pCUmL Concentration IE·16 9E·t4 1.76E+00 tE·t6 3E·14 1.57E+OO tE·t6 9E·13 S.56E·02 2E·t5 6E·t3 6.78E·Ot L.L.D: Emuent Cone.· % Emuent pCVmL pCUmL Concentration IE·16 9E·t4 9.35E·01 IE·16 3E·14 9.32E·01 tE·16 9E·13 I.46E·02 2E·15 6E·13 t.I 3E+00 Page 3 of 23 EN:RGY I ,\HOf,,\I( fill ' www.energylab.com ___ ,152 H,."" MT 877-472-071 1 • Billings, MT 808-735-«19 • Casper, WY 888-235-0515 GIII.tt., WY 866-686-7175 • Rapid City, SD 888-672-1225 • ColI.g. Station, TJl 888-6iO-221S LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter BHV Air Cl0l00417-001 Client Sample 10: BHV-l Analysos TRACE METALS Uranium, Activity RAD10NUCLIDES -TOTAL Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Roport Definitions: Rl -Analyte reporting limit. aCL -Quality control limit. Result 115 S30 15 S.7 18.0 I .S 0.8 38 7.0 O.SS Unit. pCVFilier pCi/Filler pCI/Fliter pCVFilter pCilFiller pCilFilter pCi/Filter pCi/Filter pCi/Filter pCi/Filter MOC -Minimum detectable concentration Qualifiers Rl 0.2 Report Date: 12106/10 Collection Date: 10104/10 DateRecelved: 10108/10 Matrix: Filter MCll QCl Mothod Analysis Dato / By SW6020 11/03/1021 :36/ sml ESOS.OM 11/2S/10 08:11 / eli-cs ESOS.OM 11/2S/10 08:11 / eli-cs ESOS.OM 11/2S/10 08:11 / eli-cs ES03.0 11/0211023:47 / jb ES03.0 1110211023:47/ jb ES03.0 1110211023:47/ jb ES07.0 10/27/10 16:54 /dmf ES07.0 10/27/1016:54 / dmf ES07.0 10/27/1016:54 / dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 23 EN:RGY I A --\('I " I ( PI " www ... eriYIab.com AMI1fIcoI Ex __ "51 H,I,na, MT 817·472·0711 • 8111101', MT 800·735·4489 • CBSper, WY 888·235·051 5 GiII,tt" WY 866·686·7175 . Rapid City, SO 888·672·1225 . ColI'I' Sialioo, IX 888·690·2216 ruGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: December 6, 2010 PROJECT: 3rd Quarter nHV Air SAMPLE!D: BHV.2 QuarterlDate Sampled Concentration Air Volume Radlonuclide ~CVmL C I 0040255·002 ~'U 5.47E·16 First Quarter 20 I 0 ''''Th 1.42E·17 Air Volume in mL., ""Ra 4.66E·17 1.36E+11 210Pb S.24E·15 QuarterlDate Sampled Concentration Radionuclide Air Volume ~CVmL Cloo7033S·oo2 ~'U 3.5SE·16 Second Quarter 20 I 0 ""Th 6.64E·17 Air Volume in mLs 226Ra 9.90E·17 1.36E+1 1 210Pb 2.0IE·15 QuarterlDatc Sampled Concentration Radlonucllde Air Volume ~CllmL CI0100417·oo2 M'U 2.9IE·16 Third Quarter 20 10 ""Th 4.4SE·17 Air Volume in mLs ""Ra 5.72E·17 1.37E+11 210Pb 1.0SE·15 +LLD's are from Reg. Guide4.14 Counting Precision ~CllmL NIA IE·17 4E·IS SE·17 Counting Precision ~CllmL NIA IE·17 IE·17 5E·17 Counting Precision ~CllmL NIA IE·17 9E·IS 4E·17 *Ertluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Y car for Thorium-230 Week for Radium~226 Day for Lead-210 MDC ~CllmL NIA 5E·IS 2E·IS 5E·17 MDC ~CVmL NIA 5E·IS 6E·IS 6E·17 MDC ~CllmL NIA SE·IS 5E·IS 4E·17 L.L.D.+ Emuent Cone.· % Emuent ~CllmL ~CllmL Concentration IE·16 9E·14 6.07E·01 IE·16 3E·14 4.72E·02 IE·16 9E·13 5.ISE·03 2E·15 6E·13 1.37E+00 L.L.D.+ Emuent Cone.-% Emuent ~CllmL ~CllmL Concentration 1E·16 9E·14 3.97E·01 IE·16 3E·14 2.2IE·01 IE·16 9E·13 I.IOE·02 2E·15 6E·13 3.35E·01 L.L.D'+ Emuent Cone.· % Emuent ~CllmL ~CllmL Concentration IE·16 9E·14 3.23E·01 IE·16 3E·14 1.49E·01 IE·16 9E·13 6.36E·03 2E·15 6E·13 1.79E·01 Page 5 of 23 EN:RGY AI,OII,\]CI'1i rm" W'tWt.enero1ab.com ---,'" He~na, MT 877-472-0711 • Billings, MT 801-735-4419 • Casper, WI 888-235-0515 Gill,H., WI 116-686-7175 • Rapid City, SD 888-612-1225 • ColI.g. Stallon, TJl888-690-2218 LABORATORY ANALYTICAL REPORT Cllenl: Projeel: Lab 10: Denison Mines USA Corp 3rd Quarter BHV Air Cl0l00417-002 Cllenl Sample 10: BHV-2 Analyse. TRACE METALS Uranium, Activity RADIONUCLIDES -TOTAL lead 210 Lead 210 precision (±) lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MOe Report Definitions: RL • Analyte reporting limit. ael· Quality control limit. Result 39.7 147 5.2 5.6 7.B 1.2 0.7 6.1 2.0 1.1 Units pCVFilter pCVFilter pCVFilter pCi/Filter pel/Filter pCilFilter pel/Filter pCilFilter pCVFilter pCVFilter MOe · Minimum detectable concentration Qualifiers Rl 0.2 Report Date: 12106/10 Collection Date: 10104/10 DateReeeived: 10108/10 Matrix: Filter MCll QCl Method Analysl. Date / By SW6020 11 /03/1021 :40 I sml E909.0M 11/29/10 14:45 /ell-cs E909.0M 11 /29/10 14:45 /ell-cs E909.0M 11/29/10 14:45/ ell-cs E903.0 11 /02110 23:47/ jb E903.0 11 /0211023:47/ jb E903.0 11 /0211023:47/ jb E907.0 10/27/1016:54 / dmf E907.0 10/27/10 16:54/dmf E907.0 10/27/10 16:54/dmf Mel -Maximum contaminant level. NO -Not detected al the reporting limit. Page 6 of 23 EN:RGY • f\ , 'I /d' 1'1 . WtNt.energylab.com AIII/7IfcIII Ex..-_ II!! Helena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WI 888-235-0515 Gillette, WI 8&6-686-7175 • R.pld City, SD 888-672-1225 • ColI'ge St.tion, IX 888-690-2218 mGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: December 6, 2010 PROJECT: 3rd Quarter DHV Air SAMPLE ID: BHV-4 QuarterlDate Sampled Concentration Air Volume Radionuclidc ~CVmL C10040255-003 ~'U 6.0IE-15 First Quarter 20 I 0 ''''TIt 1.26E-16 Air Volume in mLs 226Ra 1.34E-16 1.36E+11 1lOPb 1.19E-14 QuarterlDate Sampled Concentration Air Volume Radionucllde ~CVmL C10070338-OO3 ~U 2.33E-15 Second Quarter 20 I 0 ''''TIt 7.29E-16 Air Volume in mLs 226Ra 2.66E-16 1.35E+11 2]OPb 3.27E-15 QuarterlDate Sampled Concentration Air Volume Radlonuclide ~CVmL C 10 100417 ·003 ~'U 4.77E-15 Third Quarter 2010 ""TIt I.S0E-15 Air Volume in mLs m Ra S.23E-16 1.1 6E+11 210Pb 5.IIE-15 +LLD's are from Reg. Guide 4.14 Counting Precision ~CVmL N/A 2E-17 6E-18 IE-16 Counting Precision ~ClImL N/A 7E-17 2E-17 6E-17 Counting Precision ~CVmL N/A 3E-16 5E-17 SE-17 ·Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium·226 Day for Lead-210 MDC~ClImL N/A 4E-1 8 2E-18 5E-17 MDC~CVmL N/A 5E-18 6E-18 6E-17 MDC~ClImL N/A IE-17 IE-17 5E-17 L.L.D.+ Emuent Cone.· % Emuent ~CVmL ~ClImL Concentration IE·16 9E-14 6.67E+OO IE-16 3E-14 4.19E-OI IE-16 9E-13 1.49E-02 2E-15 6E-1 3 1.99E+OO L.L.D.+ Emuent Cone.· % Emuent ~CVmL ~CVmL Concentration IE-16 9E-14 2.59E+OO IE-16 3E-14 2.43E+OO IE·16 9E-13 2.96E-02 2E-15 6E-13 5.45E-OI L.L.D.+ Emuent Cone.· % Emuent ~ClImL ~CVmL Concentration IE-16 9E-14 5.30E+OO IE-16 3E-14 6.01E+OO IE-16 9E-13 9.14E-02 2E-15 6E-13 S.52E-OI Page 7 of 23 E~RGY At ,OJ Ii' J ( T'I' YfflW'.energyiab.com __ Sbfu'151 He~na, MT 877-472-0711 • Billings, MT 801-735-«89 . Casper, WI 888-235-0515 Gillette, WI 8&6-686-7175 • R.pld C~, SD 988-672-1225 • College SI.llon, IX 888-69D-2218 LABORATORY ANALYTICAL REPORT Client: Project: lab 10: Denison Mines USA Corp 3rd Quarter SHV Air C10100417-003 Client Sample 10: SHV-4 Analyse. TRACE METALS Uranium, Activity RADIONUCLIDES -TOTAL lead 210 Lead 210 precision (±) lead 210 MDe Radium 226 Radium 226 precision (±) Radium 226 MOe Thorium 230 Thorium 230 precision (±) Thorium 230 MOe Report Definitions: RL • Analyte reporting limit. QeL • Quality control limit. Result 552 591 9.1 6.0 95.2 5.2 1.1 209 31 1.4 Units pei/Fitter pel/Filler pel/Filler pel/Filter pei/Filter pei/Filter pel/Filter pel/Filter pel/Filter pel/Filter MOe· Minimum detectable concentration Qualifiers Rl 0.2 Report Date: 12106/10 Collection Date: 10/04/10 DateRecelved: 10/08/10 Matrix: Filter MCL! QCl Method Analysis Date / By SW6020 11/03/1022:01/ sml E909.0M 11 /29/10 16:56 /ell-cs E909.0M 11 /29/10 16:56 /ell-cs E909.0M 11 /29/10 16:56/ell-cs E903.0 1110211023:47/ jb E903.0 1110211023:47/ jb E903.0 11/0211023:47 / jb E907.0 10/27/1016:54/ dmf E907.0 10/27/1016:54/ dmf E907.0 10/27/10 16:54 /dmf MeL· Maximum contaminant level. NO • Not detected at the reporting limit. Page 8 of 23 EN:RGY 1\ ,(~I'/<I' I~I • www.energylab.com AMI)tIeIII ru-.. S/m:. lISt Helena, MT 877·472·0711 • Billings, MT 800·735·4489 • Casper, WY 888·235·0515 Gillette, WY 866·686·7175 • Rapid City, SO 888·&72·1225 • College SI.lIon, IX 888·690·2218 HIGH YOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: December 6, 2010 PROJECT: 3rd Quarter BUV Air SAMPLE 10: BHY.S QuartcrlDate Sampled Radionucllde Concentration Air Volume pCVmL C I oo402SS·004 nalV 4.78E-IS First Quarter 20 I 0 ""Th 3.73E·16 Air Volume in mLe; "'Ra 4.19E·16 1.36E+tt 210Pb 1.30E·14 Quarter/Date Sampled Concentration Radionuclide Air Volume pCVmL C I 0070338·004 ~'U 4.3SE·IS Second Quarter 201 0 ""Th 7.84E·16 Air Volume in mLs 226Ra l.OSE·IS 1.36E+II 210Pb 4.40E·IS Counting Precision pCVmL N/A 4E·17 IE-J7 IE·16 Counting Precision pCVmL N/A 7E·17 4E·17 7E·17 QuarterlDate Sampled Concentration Counting Air Volume Radlonucllde pCVmL Cto100417·oo4 ~'U 3.S7E·tS Third Quarter 2010 ""Th 1.I4E·tS Air Volume in mts 226Ra 7.97E·t6 l.03E+11 210Pb 3.78E-tS +LLD's are from Reg. Guide 4.14 ·Efnuent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natura1 Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 Precision pCVmL N/A 2E·t6 3E-t7 7E-t7 MDC pCVmL N/A 6E·18 2E·18 SE·J7 MDC pCVmL N/A 7E·18 6E·18 6E·t7 MDCpCVmL N/A 2E-t7 SE-t8 6E-t7 L.L.D.+ Emuent Cone.· % Emuent pCVmL pCVmL Concentration IE-16 9E-14 S.31E+00 IE·16 3E·14 l.24E+00 IE·16 9E·13 4.66E·02 2E·IS 6E·13 2.17E+00 L.L.D.+ Emuent Cone. * % Emuent pCVmL pCVmL Concentration IE·16 9E·14 4.83E+OO IE-16 3E·14 2.6IE+00 IE·16 9E·13 1.I6E-01 2E·tS 6E·13 7.33E-01 L.L.D: Emuent Cone.· % Emuent pCVmL pCVmL Concentration 1E·16 9E·14 3.97E+00 IE-16 3E·14 3.8tE+00 IE-16 9E-t3 8.86E-02 2E-IS 6E-13 6.30E-Ot Page 9 of 23 EN:RGY ,i'lOPi\I"UI' • www.energylab.com _-$Iou I"' He~na, MT 871-472-0111 • Billings, MT 801-735-«19 · Casper, WY 888-235-0515 Gillette, WY 816-&86-7175 · Rapid City, SD 888-&72-1225 · ColI.ge Station, TlI888-&SO-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter BHV Air Cl0l00417-004 Client Sample 10: BHV-5 Analyse. TRACE METALS Uranium, Activity RAOIONUCLIOES -TOTAL Lead 210 Lead 210 precision (±) Lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOe Thorium 230 Thorium 230 precision (±) Thorium 230 MOe Report Definitions: RL -Analyte reporting limit. aeL • Quality control limit. Result 36S 3S1 7.7 6.0 82.3 3.4 0.5 118 21 1.8 Units pei/Filter pei/Filter pei/Filter pei/Filter pei/Filter pei/Filter pel/Filter pei/Filter pel/Filter pel/Filter MOe -Minimum detectable concentration Qualifier. Rl 0.2 Report Date: 12106/10 Collection Date: 10/04/10 OateRecelved: 10/08/10 Matrix: Filter MCll QCl Method Analysl. Oate 1 By SW6020 11103/10 22:05 / sml ESOS.OM I 1I2S/10 I S:08 / eli-cs ESOS.OM I 1/2S/10 19:08/ eli-cs ESOS.OM I 1I2S/10 1S:08 / eli-cs ES03.0 11 /02110 23:471 jb ES03.0 11 /02110 23:471 jb ES03.0 1110211023:47 / jb ES07.0 10/27/10 16:54 /dmf ES07.0 10/27/10 16:54 /dmf ES07.0 10/27/10 16:54/dmf MeL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 10 of 23 EN:RGY A H I', "'In' www.energylab.com AMI1fIc>I Exc.-. SItJu 11$1 Helena, MT 817·472·0711 • BIllings, MT 800·735·4489 • Casper, WY 888·235·0515 Gillette, WY 866·686·7175 • Rapid City, SD 888·672·1225 • College St.tlon, IX 888·690·2218 HIGH YOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: December 6, 2010 PROJECT: 3rd Quarter BHY Air SAMPLE 10: BHY·6 QuarterlDale Sampled Concentration Radionuclide Air Volume pCUmL C I 0040255·005 ~U 9.63E·IS First Quarter 20 I 0 2l'Th 1.82E·16 Air Volume in mLs 226Ra 2.06E·16 1.36E+ II 2\OPb 1.37E·14 QuarterlDate Sampled Concentration Air Volume Radionuclide pCUmL C10070338·OOS ~'U 3.62E·IS Second Quarter 20 I 0 ""Th 3.94E·16 Air Volume in mLs 226Ra 4.89E·16 I.3SE+11 2\OPb 4.30E·IS QuarterlDate Sampled Concentration Air Volume Radionuclide pCUmL CIQI00417·ooS nalU S.42E·IS Third Quarter 2010 2l0Th 1.08E·IS Air Volume in mll! 226Ra S.68E·16 1.03E+11 210Pb 3.98E·IS +LLO's are from Reg. Guide4.14 Counting Precision pCUmL NIA 2E·17 7E·18 IE·16 Counting Precision pCUmL NIA 4E·17 2E·17 7E·17 Counting Precision pCUmL NIA 2E·16 3E·17 8E·17 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B · Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCpCUmL NIA 4E·18 2E·18 SE·17 MDCpCUmL NIA SE·18 SE·18 6E·17 MDCpCUmL NIA 2E·17 6E·18 6E·17 L.L.D.+ Emuent Cone. * % Emuent pCUmL pCUmL Concentration IE·16 9E·14 1.07E+01 IE·16 3E·14 6.07E·01 IE·16 9E·13 2.29E·02 2E·IS 6E·13 2.29E+00 L.L.D.+ Emuent Cone. * % Emuent pCUmL pCUmL Concentration IE·16 9E·1 4 4.02E+OO IE·16 3E·1 4 1.3 I E+OO IE·16 9E·1 3 S.43E·02 2E·IS 6E·13 7.17E·01 L.L,D.+ Emuent Cone. * % Emuent pCUmL pCUmL Concentration IE·16 9E·14 6.02E+00 IE·16 3E·14 3.6IE+00 IE·16 9E·13 6.3IE·02 2E·IS 6E·13 6.63E·01 Page 11 of 23 EN:RGY l I\Horll\ror<rr' YMW.energyiab.com __ smc.'1S2 Helena, MT 811-412-0711 • Billings, MT 800-135-4-488 • Casper, WY 888-235-0515 GiII.tt., WY 816-688-1115 • Rapid City, SO 888-612-1225 • ColI.g. Slation, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter BHV Air C10100417-005 Client Sample 10: BHV-6 Analyses TRACE METALS Uranium, Activity RADIONUCLIDES -TOTAL Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 559 411 7.8 6.0 58.6 3.0 0.6 112 20 1.8 Units pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter MOC -Minimum detectable concentration Qualifiers RL 0.2 Report Date: 12106/10 Collection Dale: 10/04/10 DaleRecelved: 10/08/10 Malrlx: Filter MCL! QCL Method Analysis Oate l By SW6020 11/03/1022:091 sml E909.0M 11129/10 21 :19/eli-cs E909.0M 11/29/1021 :19 1 eli-cs E909.0M 11/29/1021 :19 /eli-cs E903.0 11/03/1001 :331 jb E903.0 11/03/1001 :331 jb E903.0 11/03/1001 :331 jb E907.0 10/27/10 16:54/dmf E907.0 10/27/10 16:54/dmf E907.0 10/27/10 16:54/dmf MCL -Maximum contaminant level. NO -Not detected at the reporting limil. Page 12 of 23 EN:RGY I 1\-j('I,/d' 1<1 www.energy\ab.com ~fEx"~t.sl ... 7152 Helena, r.rr 877·472·0711 • Billings, r.rr 800·735·4489 • Casper, Wi 888·235·0515 Gillette, Wi 816·686·7175 • Rapid City, SD 888·672·1225 • College Station, TJ( 888·690·2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: December 6, 2010 PROJECT: 3rd Quarter DHV Air SAMPLE 10: Blank QuarterlDate Sampled Radionucllde Concentration Air Volume pCllmL C I 0040255·006 M'U 1.67E·17 First Quarter 20 I 0 ""Th ·3.03E·IS Air Volume in mLs "'Ra I.4SE·IS 1.36E+11 2JOPb 3.50E·17 Counting Precision pCllmL N/A 4E·IS IE·IS 3E·17 Note' This sample uses 136 000 000 L of air volume for comparison purposes , , QuarterlDate Sampled Concentration Counting Radionuclide Precision Air Volume pCllmL pCllmL C1007033S·OO6 ~'U 2.7 IE·17 N/A Second Quarter 2010 ""TIl ·2.63E·19 5E·IS Air Volume in mls 226Ra 9.74E·IS 4E·IS 1.36E+11 210Pb 7.47E·IS 3E·17 Note· This sample uses 136 000 000 L of Dlr volume for comparison purposes , , QuartcrlDatc Sampled Concentration Counting Radlonuclldc Precision Air Volume pCllmL pCllmL CI0100417·006 "'u 9.0IE·lS N/A Third Quarter 20 I 0 ''''Tb ·1.63E·IS 7E·18 Air Volume in mw "'Ra 1.27E·IS 4E·IS 1.36E+11 210Pb ·2.26E·17 3E·17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCpCllmL N/A 5E·IS 2E·IS 5E·17 MDCpCllmL N/A 6E·IS 5E·IS 6E·17 MDCpCllmL N/A IE·17 7E·IS 4E·17 L.L,D,+ Effluent Cone.· % Emuent pCllmL pCllmL Concentration IE·16 9E·14 I.S6E·02 IE·16 3E·14 ·1.0IE·02 IE·16 9E·13 I.64E·04 2E·15 6E·13 5.S3E·03 L,L,D,+ Emuent Cone.· % Emuent pCllmL pCllmL Concentration IE·16 9E·14 3.02E·02 IE·16 3E·14 ·S.75E·04 IE·16 9E·13 I.OSE·03 2E·15 6E·13 1.24E·03 L.L.D.+ Emuent Cone.· % Emuent pCllmL pCllmL Concentration IE·16 9E·14 l.ooE·02 IE·16 3E·14 ·5.44E·03 IE·16 9E·13 1.4IE·04 2E·15 6E·13 ·3.76E·03 Page 13 of 23 EN:RGY "HOll,\ICI'i www.energylab.com AMI)1JaI--llU He~na, MT 871-472-0711 • 8l11ings, MT 801-735-4-489 • Cuper, WY 888-235-0515 Gillott., WY 856-686-7175 • R'pld City, SD 888-672-1225 • CoIl.g. SI,lion, TJ( 888-690-2218 LABORATORY ANALYTICAL REPORT Cllenl: Project: Denison Mines USA Corp 3rd Quarter BHV Air Lob 10: Cl 01 00417-006 Client Sample 10: Blank Analyse. TRACE METALS Uranium, Activity RADIONUCLIDES -TOTAL lead 210 Lead 210 precision (±) lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL • Analyte reporting limit. aCL· Quality control limit. Result 1.2 -3 3.6 6.1 0.2 0.6 0.9 -0.2 0.97 1.3 Units pCVFilter pCVFilter pCi/Filter pel/Filter pel/Filter pel/Filter pel/Filter pei/Filter pei/Filter pCl/Filter MDe • Minimum detectable concentration Report Date: 1210611 0 Collection Dale: 1010411 0 DateRecelved: 1010811 0 Matrix: Filter MCll Qualifiers Rl QCl Method Analysis Oate I By 0.2 SW6020 11/03/10 22:131 sml U E909.0M 11129/10 23:311 eli-cs E909.0M 11129/1 0 23:31 I eli-cs E909.0M 11129/1 0 23:31 I eli-cs U E903.0 1110311001 :331 jb E903.0 1110311001 :331 jb E903.0 1110311001 :331 jb U E907.0 10/27110 16:551 dmf E907.0 10/27110 16:551 dmf E907.0 10/27110 16:55/dmf MeL· Maximum contaminanllevel. ND • Not detected al the reporting limit. U . Not detected at minimum detectable concentration Page 14 of 23 EN:RGY I "HUH"I ( I'll • www.energytab.com MIIytIaJ ~ SIJIu 1m H.len., MT 817-412-0111 • BIlling., MT 80D-735-4489 • Cosper, WY 888-235-0515 Gillett., WY 816-686-7175 • R.pld Ci1y, SO 888-672-1225 • ColI.g. SI.llon, IX 888-690-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: 3rd Quarter SHV Air Analyle Count Result Units Method: E903_0 SamplalO: Cl0l00240-001AMS Radium 226 samplalO: CtOl0024D-001AMso Radium 226 samplalO: Cl0l00240-002AOUP Radium 226 Radium 226 precision (±) Radium 226 MOe Sample 10: LCs-27771 Radium 226 Sample 10: MB-27771 Radium 226 Radium 226 precision (±) Radium 226 MOe Qualifiers: RL . Analyle reporting limit. Sample Matrix Spike 59.9 pel/Filler Sample Malrlx Spike Dupllcale 56.0 pel/Filler 3 Sample Duplicate 2.19 pel/Filler 0.873 pel/Filler 0.919 pel/Filler Laboratory Control Sample 14.0 pel/Filter 3 Melhod Blank -0.1 pel/Filter 0.2 pel/Filter 0.4 pel/Filter MOe· Minimum detectable concentration Report Date: 12106/10 Work Order: Cl0l00417 RL %REC Low Limit High Llmll RPO RPOLlmlt Qual Run: BERTHOLD 770-1_101027A 116 70 130 Run: BERTHOLD 770-1 101027A 108 70 130 6.8 Run: BERTHOLD 770-1 101027A - 22 Run: BERTHOLD 770-1_101027A 94 70 130 Run: BERTHOLD 770-1_101027A NO . Not detected at the reporting limit. U -Not detected at minimum detectable concentration Balch: R139385 11/02/1021 :56 11102/10 21 :56 26.8 11/02/1021 :56 79.3 11/02/1023:47 11/02/1023:47 U Page 15 of 23 EN:RGY I "Hl)P, I ( 1<1' ,- www.energylab.com AM/ytItM ExuIIwa SbIu 1m He~na, MT 877-112-0711 • 811l1ngs, MT 800-135-«89· Cosper, WI 888-235-0515 Gillette, WI 81&-&88-7115 • Rapid City, SO 888-&72-1225 • College Stetion, IX 888-&90-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: 3rd Quarter BHV Air Analyle Count Result Units Method: E907.0 Sample lD: Cl0l00417-006AMS Thorium 230 SamplelD: Cl0l00417-006AMSD Thorium 230 SamplelD: LCS-27878 Thorium 230 SamplelD: MB-27878 Thorium 230 Thorium 230 precision (±) Thorium 230 MOe Qualifiers: RL . Analyte reporting limit. 3 MDC . Minimum detectable concentration Sample Matrix Spike 56.2 pCi/Filier Sample Matrix Spike Duplicate 56.9 pCi/Filier Laboratory Control Sample 3.81 pCilFilter Melhod Blank -0.2 pCi/FilIer 0.1 pCilFilter 0.2 pCilFilier Report Date: 12106/10 Work Order: Cl0100417 RL %REC Low Limit High Limit Run: EGG-ORTEC_l01025B 116 70 130 Aun: EGG-OATEC_l0l025B 120 70 130 Run: EGG-OATEC_l0l025B 83 70 130 Run: EGG-ORTEC_l 0l025B NO . Not detected at the reporting limit. RPD RPDLlmlt Qual 1.2 Balch: 27878 10/27/10 16:55 10/27/10 16:55 51.7 10/28/1009:34 10/28/10 09:34 U U • Not detected at minimum detectable concentration Page 16 of 23 EN:RGY I AHUllAlel'll '0 www.energylab.com AMtytaI Exe"""" ShJU ,m He~", MT 877-472-0711 • Billings, MT 800-735·4489 · C3SPor, WY 888-235-0515 Gillette, WY 866-686-7175 • Repld City, SD 888-672-1225 • College SI,lion, TJ( 888-680-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: 3rd Quarter BHV Air Analyte Count Result Units Method: E909.0M SamplelD: MB-12622 /27878 Lead 210 Lead 210 precision (±) Lead 210 MDC Sample 10: LCS-12622 /27878 Lead 210 3 Method Blank 0.08 pCi/L 4 pCi/L 6 pCi/L Laboratory Control Sample 43 pCi/L Report Date: 12/06/10 Work Order: Cl0l00417 RL %REC Low Limit High Limit Run: SUB·T37900 Run: SUB-T37900 19 70 130 RPD RPDLlmlt Qual Balch: T _PB·21 0·0044 1112911003:48 U 11/29/1006:00 S -leS response is outside of the acceptance range for this analysis. Since the MS, MSD, and second LeS are acceptable the batch is approved. Sample 10: TtOl00081·001AMS Lead 210 Sample Matrix Spike 2570 pCi/Filler Run: SUB·T37900 150 70 130 11/29/1010:22 S • Sample response is much targer than spike amount, therefore small variances in the sample adversely affected the recovery. The second LeS and the RPD of the MSIMS[ pair meels acceptance criteria; this batch is approved. Sample 10: Tl0l00081-001AMSO Sample Malrix Spike Duplicale Lead 210 2330 pCi/Filter Sample 10: MB-12669 /27996 Lead 210 3 Melhod Blank Lead 210 precision (±) Lead 210 MDC Sample 10: LCS-12669 /27996 Lead 210 Qualifiers: RL· Analyte reporting limit. MOe -Minimum detectable concentration ·2 pCi/L 4 pCi/L 7 pCi/L Laboratory Control Sample 220 pCi/L U -Not detected at minimum delectable concentration 129 Run: SUB· T37900 70 Run: SUB·T37900 Run: SUB·T37900 130 94 70 130 NO -Not detected at the reporting limit. S -Spike recovery outside 01 advisory limits. 9.9 11/29/1012:34 13.5 11/30/10 21 :24 U 11/30/10 23:36 Page 17 of 23 EN:RGY I 1\11()ji, I' 1<1' www.energylab.com ___ ,m He~na, MT 871-472-0711 • Billings, MT 800-735-4489 . Cuper, WY 888-235-0515 GIII,tte, WY 1IS-688-7175 • R,pld City, so 888-672-1225 • Colleg, St,tion, n 888-690-2218 Client: Denison Mines USA Corp Project: 3rd Quarter BHV Air QA/QC Summary Report Report Date: 12106/10 Work Order: Cl0l 00417 Anatyta Count Result Units RL %REC Low Limit High Limit RPD RPDLlmlt Qual Method: SW6020 SamptelD: MB-27878 Uranium Sample ID: LCS2-27878 Uranium SamplelD: Cl0l00587-007AMS Uranium Sample tD: Cl0l00587-007AMSD Uranium Qualifiers: RL · Analyte reporting limit. MOe· Minimum detectable concentration Method Blank Run: ICPMS2-C_'0"03A 0.0003 mg/filler 6E-05 Laboratory Control Sample Run: ICPMS2-C_'0"03A 0.102 mglfilter 0.00030 101 85 115 Sample Matrix Spike Run: ICPMS2-C_'0"03A 1.B7E-08 mglfilter 0.00030 101 75 125 Sample Matrix Spike Duplicate Run: ICPMS2-C_' 01 1 03A 1.B7E-08 mg/filler 0.00030 101 75 125 NO . Not detected at the reporting limit. Batch: 27878 11/03/1021 :20 11/03/1021:24 11/03/1023:03 11/03/1023:07 20 Page 18 of 23 EN:RGY 1\ l"li/\jr .'1 Helena, MT 877·412·0111 • Billings, MT 800·135·4489 • Casper, WI 888·235·0515 GIII.tt., WI 166·686·1115 • R.pld City, SD 888·612·1225 • ColI.g. Station, III 888·690·2218 Workorder Receipt Checklist Denison Mines USA Corp 1111I~llIlilllllll C10100417 Login completed by: Edith McPike Reviewed by: BL2000lkschroeder Reviewed Date: 10/15/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 ·c NA Yes D Yes D Date Received : 10/8/2010 Received by: tae Carrier name: NDA No D No D No D No D No D No D No D No D No D No D Not Present D Not Present 0 Not Present 0' No D No D No VOA vials submitted 0' Not Applicable 0 Page 19 of 23 Chain of Custody and Analytical Request Record ,N). ~ t.JfIc" _)J ,JilIJ Report Mail Ad~ess: C-<; t ',0 (5-:« .:> C'I !]:, ~ &'~I 1/1. L fii 4:;'/ I Invoice Address: I ..... ,,~.~ PLEASE PRINT Provide as much information as Project Njme, PWS, Permit, Etc, , S (l.. (Ju:. m fL .J~ J.W A.112. {A I __ ... __ Name: Email: l2, tvJ a!v.-t~ i1-%' --"'7"7/ Invoice Contact & Phone: rI.lII.,;IIQ.,8 Order: ,~..-.L page-L of +- Yes @/ No 0 Sampler: (Please Print) '72q~ '~""'''''Ule Order: Special Report/Formats: ~ ... 1 Contact ELI prior to """'t't' ..... uy. RUSH sample submittal &G&l\ll, '\7@(]@ OO@:®(]!)~~ Dow D POTWfWWTP D State: ___ _ D Other: ___ _ D EOO/EOT(Electronlc Data) Format: D LEVEL'7.'IV-,.---- D NELAC o ~ ~o <I> ~m;g51 ~ fj> 0 >.2 f5(1)~ ~ ~ u!:"o CIJ Q) o<~~I~ ... 8.* §C3 ~~r'lii ' j~'~Ia; ;;: Z a.<l. ~c ~ >1 en ~~~~ r-~S~AM~P~L~E~ID~E~N~n~F~IC~A~T=IO~N~,-~~--~~--~~----~ ~ (Name, Location, Interval, etc,)_ . '1?J+iI-J ~I ;VA -I 2{SJtil-2 '-rJ,JW-'4 I I l'lsHv·j: 1~/1 f'hf4' 10 I /VCr I'" 11J~ / ( } ( B-A for charges and c 0 !:;: R scheduling -See ~ W t:. Instruction Page ::c u () " Comments: ::> U « e I-ro ~ " 5 .... S W 'E Custody Seal W ro (/) '0 " c7l H i ~ . ~ o 9 ~ ~ ,. ~~v~/7 ~ Custody R ' . by (Pt!! L .~"emme II(jO ] 7'""?" I j Roce""",y(pri"l: OatefTime: S;gn ..... : o I::::;;'''''AJ .... IIF1 ,7fiitJ ~ , II/~' ~ :~~r:e R"mq."""" by (pnnl, Oolemme: "/ '~nr'": R"",,,,,,, by (pri"'l: ootemme: S9>'tu~ . r 0<0, <aN"" u"~,,me I' V/ c /,' 9. ~'~A. ,'~ ~..I_ Signed SamoieDisposal, Returnto Chent LabDlsP05al '/6 /Ill ,:Yj/I!L ,~I In certain circumstances, samples submitted to Energy Laboratones, Inc. may be subcontracted to other certified laboratones in order to ~omplete the a~ request~ This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee SChedule. forms, and links. Period: July 5,2010 through October 4, 2010 (3rd Quarter 2010) Page' BHV-l on stream % 100.2% BHV-1 Total Volume: 4.83E+06 Week Filter Start St"" St"" Start Total Total loading, Per Cent · ...... , ....... ...... , .. !.Ia, .. ...'v ..... ... '., , .... . .. " .. .,,"" '''', .. ............... '" """' .................. " ........ ' ,., 1 8155038 5-Jul-1O 12·1u1-JO 4.6330 4.4509 0.1821 22305.0 22135.0 10201.2 10,543,602 0.0173 101.2% 36.5 , 8155031 12-Jul·lO 19·JuJ.IO 4.6548 4.4684 0.1864 22474.1 22305.0 10143.6 10.627.686 0.0175 100.6% 37.0 , 8155026 I9-Jul-lO 26-Jul·1Q 4.6658 4.4863 0.1795 22641.7 22474.1 10060.8 10.540,935 0.0170 99.8% 37.0 4 8155015 26-Ju1-10 2·Aug·1O 4.6143 4.4842 0.1301 22806.6 22641.0 9937.8 10.4IU165 0.0125 98.6% 37.0 5 8155012 02·Aug-1O 9·Aug·1O 4.5842 4.4939 0.0903 22998.1 22806.6 11485.2 12.033.312 0.0075 113.9% 37.0 6 8155006 09-Aug'lO 16·Aug·10 4.6506 4.4953 0.1553 23145.8 22998.1 S865.6 9.288,696 0.0167 88.0% 37.0 7 8153799 16·Aug·IO 2~·Aug·10 4.fiJ67 4.4682 0.1385 23310.8 23145.8 9897.6 10.341,920 0.0134 98.2% 36.9 8 8153793 23·Aug·1O ~Aug·IO 4.6648 4.4809 0.1839 23478.4 23310.8 10054.8 10.506.177 0.0175 99.7% 36.9 9 8153784 3O-Aug-IO 6-Sep-l0 4.7252 4.4974 0.2278 23761.6 23478.4 16997.4 17.760.441 0.0128 168.6% 36.9 10 8153778 06·Sep-1O 13·Sep·10 4.5427 4.4899 0.0528 23812.3 23761,6 3039.6 3,150,231 0.0168 30.2% 36.6 11 8153772 13-Sep-IO 20-Scp-1O 4.7300 4.4993 0.2307 24027.9 23812.3 12934.8 13,332.328 0.0173 128.3% 36.4 12 8153769 20-Scp-JO 27-Sep-IO 4.5843 4.4992 0.0851 24148.3 24027.9 7224.6 7,446,635 0.0114 71.7% ,6.4 " 8153763 27-Sep-10 4-OcI-lO 4.7094 4.4890 0.2204 24322.8 24148.3 10469.4 1O.79L158 0.0204 103.9% '6.4 TotaL<; 91 2184.0 4.6435231 4.484&385 0.1587 1313[2.4 I 36,n5.188 0.0152 100.2% 36.8 BHV·2 on stream % 100.0% BHV·2 Total Volume: 4.B2E+06 Week Filter Start St"" St"" Start Total Total loading, PerCent • Number Date Date Gmss Tare Net Time Time Time Liters mQ/m3 1 8155037 05-Jul'10 2 8155030 12.Jul·l0 3 8155025 19-Jul·l0 26·Jul-l0 4.7560 4.5055 0.2505 32830.4 32663.0 10042.8 10,522,076 0.0238 99.6% 37.0 4 8155016 26.Jul-l0 02·Aug-10 4.7152 4.5019 0.2133 32995.9 32830.4 9928.2 10,402,007 0.0205 98.5% 37.0 5 8155011 02·Aug·l0 09·Aug-l0 4.6878 4.4792 0.2086 331 87.1 32995.9 11473.2 12,020.739 0.0174 113.8% 37.0 6 8155005 Og..Aug·l0 IS·Aug·tO 4.8159 4.4915 0.3244 33334.8 33187.1 8863.8 9,286,810 0.0349 87.9% 37.0 7 6153798 16-Aug-l0 23·Aug-l0 4.8275 4.5056 0.3219 33500.7 33334.8 9954.6 10,401,478 0.0309 98.8% .36.9 8 8153792 23-Aug-l0 30-Aug-l0 5.0157 4.4924 0.5233 33667.5 33500.7 10006.8 10,456.022 0.0500 99.3% '6.9 9 8153785 , 30-Aug-10 OS-Sap' to 5.0077 4.4786 0.5291 33860.0 33667.5 11552.4 12,071,006 0.0438 114.6% 36.9 10 8153779 06-Sep-l0 13-Sep-l0 4.6158 4.4789 0.1369 34001.3 33860.0 8477.4 8,785.949 0.0156 84.1% .36.6 11 8153773 13..sep·10 20·5ep-10 4.9615 4.4748 0.4867 34216.9 34001.3 12937.2 13,334.802 0.0365 128.3% .36.4 12 8153768 20·59p-10 27-Sep-10 4.6552 4.4955 0.1597 34337.3 34216.9 7222.2 7,444,162 0.0215 71.6% 36.4 13 8153762 27-Sep-l0 O4-Oct·l0 4.9986 4.4956 0.5030 3450S.1 34337.3 10307.4 10,624.180 0.0473 102.3% 36.4 Totals 91 2184.0 4.8395 4.48647 0.3530 131096.4 136.505,628 0.0331 100.0% '6.8 8HV·4 on stream % 84.7% BHV-4 Total Volume: 4.08E+06 Week Filter $Iart St"" Stop Slart Total Total loading. Per Cent • Number Date Da .. Gross Ta", Net Time Time Time Uters malm3 On Stream SCFI 1 8155036 OS.Ju1-10 12-Jul·l0 4.7590 4.4963 0.2627 7982.8 8149.1 -9978.0 (to.312.S11) ·0.0255 -99.0% 36~ 2 8155029 12·Ju1-1Q 19-Jul-l0 4.8849 4.4824 0.4025 8319.0 8149.1 10194.0 10,680,492 0.0377 101.1% 37.0 3 8155024 19.Jul·l0 26.Jul-l0 4.8615 4.4440 0.4175 8487.5 8320.0 10053.0 10,532,763 0.0396 99.7% ]7.0 4 8155017 26-Jul·1Q 02-Aug-l0 4.7460 4.5116 0.2344 8654.6 8487.5 10018.4 10.506.989 0.0223 99.5% 37.0 5 8155010 02-Aug-10 09-Aug-tO 4.7151 4.5039 0.2112 8842.9 8654.6 11295.0 11.834.035 0.0178 112.1% 37.0 6 8155004 09-Aug·10 16-Aug-l0 4.7384 4.5081 0.2303 8990.8 8842.9 8872.8 9.296,240 0.0248 88.00/0 ]7.0 7 8153797 16-Aug-l0 23·Aug-10 4.7419 4.5091 0.2328 9155.9 8990.8 9904.8 10,349,443 0.0225 98.3% .36.9 8 8153791 23-Aug-l0 30-Aug-l0 4.7888 4.5037 0.2851 9323.7 9155.9 10071.0 10,523,104 0.0271 99.9% 36.9 9 8153786 3O-Aug·l0 06-Sep-l0 4.7040 4.4731 0.2309 9515.6 9323.7 11 515.2 12,032,136 0.0192 114.2% 36.9 to 8153780 06-Sep-l0 13-Sep-10 4.6258 4.4941 0.1317 9657.3 9515.6 8500.2 8,809,578 0.0149 84.3% 36.6 " 8153774 13-Sep-tO 2f)-Sep-l0 4.8868 4.4816 0.4052 9871.8 9657.3 12870.0 13,265,537 0.0305 127.7% 36.4 12 8153767 2Q-Sep-l0 27-Sep-10 4.5147 4.4810 0.0337 9993.5 9871.8 7299.6 7,523,940 0.0045 72.4% ]6,4 "U Ql '" CD N N 9. N W Week . 1 2 3 4 5 6 7 8 9 10 11 12 13 SHV-5 on stream % Fitter Slart .-~." .... ~ . -........ 8155035 05-Jul-10 8155028 12-Jul-l0 8155023 19-Jul-l 0 8155019 26-Jul-l0 8155009 02'Aug-l0 8155003 09-Aug-10 8153796 16-Aug-l0 8153790 23-Aug·l0 8153787 3D-Aug-l0 8153781 06-Sep-l0 8153775 13-Sep-tO 8153766 20-Sep-l0 8153760 27-Sep-l0 Totals 91 75.4% SlOP ....... ~ .....'" ...... , .. ,~ ..... , 12-Jul-10 4.6790 4.4594 0.2196 19-Jul-10 4.7034 4.4781 0.2253 26-Jul-l0 4.7470 4.5127 0.2343 02-Aug-l0 4.6643 4.4908 0.1735 09·Aug-l0 4.6053 4.4989 0.1064 16-Aug-l0 4.6559 4.4959 0.1600 23-Aug·l0 4.6362 4.4853 0.1509 30·Aug-l0 4.6685 4.4782 0.1903 06-Sep-l0 4.7436 4.4836 0.2600 13-Sep-l0 4.5538 4.5207 0.0331 2O-Sep-l0 4.51 i6 4.4976 0.0140 27-Sep-l0 4.5082 4.5082 0.0000 04-Oct-l0 4.6416 4.4786 0.1630 2184.0 4.63988 4.49138 0.1485 BHV-5 Total Volume: 3.64E+06 Stop Start Total Total Loading, Per Cent .,," ... '''" ... '"'''''' ..... "' .... '" " .... '-'"" ........... '" ........ ' 'w, 32446.0 32279.5 9991.2 10,326,554 0.0213 99.1% 36.5 32616.9 32446.0 10251.0 10,740,212 0.0210 101.7% 37.0 32784.4 32616.9 10053.6 10,533,391 0.0222 99.70/0 37.0 32951.3 32784.4 10012.2 10,490,016 0.0165 99.3% 37.0 33140.4 32951.3 11345.4 11.886,840 0.0090 112.6% 37.0 33288.2 33140.4 8867.4 9,290,582 0.0172 88.0% 37.0 33453.3 33288.2 9906.0 10,350,697 0.0146 98.3% 36.9 33620.5 33453.3 10036.2 10,486,742 0.0181 99.6% 36.9 33812.2 33620.5 11497.2 12,013,328 0.0216 114.1% 36.9 33842.9 33812.2 1841.4 1,908,421 0.0173 18.3% 36.6 33842.9 33842.9 0.0 0 #DIV/OI 0.0"10 36.4 33842.9 33842.9 0.0 0 IDIV/a! 0.0"10 36.4 33927.2 33842.9 5£X>2.2 5,217,778 0.0312 50.2% 36.4 7?~~ _98~.~ ~,?44,560 #DIVlO! 75.4% 36.8 -u 1\l co CD '" W o -'" W Week " I 2 3 4 5 6 7 8 9 10 11 12 13 Week 2 3 4 5 6 7 8 9 10 11 12 Period: July 5, 2010 through October 4, 2010 (3rd Quarter 2010) SHV-6 on stream % 75.4% Filter Start Slop Slop , ... ,', ...... , """'." .... "" ... .....'v""'" ,e,,,, .. "" '''''''' 8155034 05-Jul-10 12-Ju1-10 4.6746 4.4789 0.~957 9498.6 8155027 12-Jul-10 19-Ju1-10 4.7025 4.4543 0.2482 9669.5 8155022 19-JuJ-10 26-J u1-10 4.7134 4.4978 0.2156 9837.1 8155020 26-Jul-l0 02-Aug-l0 4.6755 4.5018 0.1737 10003.8 8155008 02-Aug..10 09-Aug-l0 4_6356 4.5167 0.1189 10192.5 8155002 09-Aug-10 16-Aug-10 4.6561 4.4915 0.1646 10340.4 8153795 16-Aug-10 23-Aug-10 4.6396 4.4867 0.1529 10505.5 8153789 23-Aug-l0 3O-Aug-l0 4.7013 4.4740 0.2273 10673.0 8153788 30-Aug·tO 06-Sep-10 4.7864 4.5060 0 . .2784 10864.7 8153782 06-Sep-tO 13-Sep-l0 4.5056 4.4742 0.0314 10895.2 8153776 13-Sep-l0 20·Sep·10 4.4895 4.4759 0.0136 10895.2 8153765 2O-Sep-l0 27-Sep-l0 4.4948 4.4945 0.0003 10895.2 8153759 27-Sep-10 04~Oct-10 4.6263 4.4918 0.1345 10979.6 Totals 91 2184.0 4.63855 4.48816 0.1504 ALL BHV on stream % 87.2% Start Slop Ie Date ",0 12-JuH 8155021 12-Jul-l0 19-Ju1-10 4.4803 8155014 19-Ju1-10 26-Jul-10 4.4772 8155013 26-Ju1-10 02-Aug-l0 4.5079 8155007 02-Aug-l0 09-Aug-10 4.5113 8153800 OS-Aug-10 16-Aug-l0 4.4861 8153794-16·Aug-l0 23-Aug·10 4.5071 8153783 23·Aug·l0 3O-Aug-l0 4.4884 8153777 3O·Aug·10 06-Sep-10 4.4S37 8153771 06-Sep-10 13-Sep-l0 4.4674 8153770 13·Sep-10 20-Sep-10 4.4826 6153764 20·Sep-l0 27-Sep-l0 4.4778 Page 2 BHV-6 Total Volume: 3.63E+06 Start Total Total Loading. Per Cent ""'.:; ,.,,"" ...... ""." '" " ..... '-"' ....... "'Q." ..... '-', .w, 9332.0 9997.8 10,333,375 0.0189 99.2% 36.5 9498.6 10255.2 10,744,612 0.0231 101.7'10 37.0 9669.5 10053.0 10,532,763 0.0205 99.7"h 37.0 9837.1 10002.6 10,479,957 0.0166 99.2% 37.0 100OS.8 11325.0 11,865.467 0.0100 112.4% 37.0 ! 10192.5 8871.0 9,294.354 0.0177 88.0% 37.0 10340.4 99060 10.350,697 0.0148 98.3% 36.9 10505.5 10049.4 10.500,534 0.0216 99.7% 36.9 10673.0 11506.2 12,022.732 0.0232 114.1% 36.9 10864.7 1825.2 1,891,631 0.0165 18.1% 36.6 10895.2 0.0 0 'DIVlO! 0.0% 36.4 10895.2 0.0 0 #DIV/O! O.OOk. 36.4 10895.2 5064.0 5.219,633 0.0258 50.2% 36.4 98855.4 103,235,758 #Otv/O! 75.4% 36.8 EN:RGY /\ll:J.,AICI<lt ~ www.energyleb.com AMIytJnI fxMJe«t SIrIc. 1152 Helena, MT 817"72-0111 • Billings, MT 800-735-«89 ' Casper, WY 888-235-0515 Gillette, WY 8&6-&86-7175 • Rapid City, SO 888-&72-1225 • College Station, IX 888-&90-2218 February 08, 201 I Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 8451 I WorkorderNo.: Cll0l 0188 Project Name: 4th Quarter BHV Air ANALYTICAL SUMMARY REPORT Energy Laboratories, Inc. Casper WY received the following 6 samples for Denison Mines USA Corp on 1/6/2011 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test Cll0l0188-001 BHV-l 01104 /1 I 00:00 01 /06/1 I Filter Composite of two or more samples Metals, Total Digestion, Total Metals Lead 210 Radium 226 Thorium, Isotopic Cl I 01 01 88-002 BHV-2 01 /04 /1 I 00 :0001/0611 I Filter Same As Above Cl I 01 01 88-003 BHV-4 01 /0411 I 00 :00 0 I 106/1 I Filter Same As Above Cl I 01 01 88-004 BHV-5 01 /04/1 1 00 :0001/06/11 Filter Same As Above Cl I 01 01 88-005 BHV-6 01104/1 I 00:00 01/06/1 I Filter Same As Above Cl I 01 01 88-006 Blank 01/04/1 I 00:00 01/06/1 I Filter Same As Above This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analyrical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted fo r testing. If you have any questions regarding these test results, please call. Report Approved By: ,~~/ /. (/fl~v=-c:~ Technical Director Dig itally signed by Steve Carlston Date : 2011.02.09 11 :10:00 -07:00 Page 1 of 22 IWIW.energylab.com AIuIytJtII ExuIJHcf!btu '151 CLIENT: Denison Mines USA Corp Project: 4th Quarter BHV Air Sample Delivery Group: Cll 01 0188 ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4'C (±2'C) MT 871-472-11711 • Billin!', MT 800-735-4489 • Casper, WY Report Date: 02/08/11 CASE NARRATIVE Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by th is method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS Th e desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of count ing should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated . ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYS IS Subcontracting of sample analyses to an outside laboratory may be required. II so, ENERGY LABORATORI ES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641 , Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in th is report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreCiates the opportunity to provide you with this analyt ical service. For additional information and services visit our web page www.energylab.com. Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. Page 2 of 22 www.energylab.com bllyticill ExcellencfJ Since '952 EN:RGY Helena , MT 871·472·0711 • Billings, MT 800·735·4489 • Casper, WY 888·235·0515 Gillette, WY 866·686·7175 ' Rapid City, SD 888·672·1225 ' College Station, TX 888·690·2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: February 9, 2011 PROJECT: 4th Quarter BHV Air SAMPLE 10, BHV·I QuarterlDate Sampled Concentration Air Volume Radionuclide pCi/mL CtOO40255-001 nOIU 1.97E-15 First Quarter 2010 'lOTh 2.15E-16 Air Volume in mls 2URa 3.27E-16 1.36E+11 2LOPb I.OOE-14 QuarterlDate Sampled Concentration Radionuclide Air Volume J.lCilmL C IOO7033S-001 ~U 1.5SE-15 Sccond Quarter 20 I 0 'lOTh 4.l IE-16 Air Volume in mls 226Ra 7.70E-16 1.36E+t t 2LOPb 4.07E-15 QuartcrlDate Sampled Concentration Air Volume Radionuclide J.lCi/mL CIOI00417-00t ~'U S.42E·16 Third Quarter 2010 'lOTh 2.S0E·t6 Air Volume in mls 226Ra 1.31E·16 1.37E+ II 2LOPb 6.S0E-15 Counting Precision J.lCilmL N/A 3E-17 9E-IS 9E-17 Counting Precision J.lCilmL N/A 5E-ll 3E-17 6E-t7 Counting Precision J.lCi/mL N/A 5E-17 IE-17 IE-16 QuarterlDate Sampled Concentration Counting Air Volume Radionuclide J.lCi/mL CIIOIOISS-OO I ~'U 1.27E-15 Fourth Quarter 20 I 0 ''''Th 2.32E-16 Air Volume in mls 226Ra 2.30E-16 1.39E+11 2LOPb 1.27E·t4 +LLD's are from Reg. Guide 4.14 *Efflucnt Concentration from the NEW 10 CFR Part 20 -Appendix B . Table 2 Year for Natural Uranium Year for Thorium·230 Week for Radium·226 Day for L..cad·210 Precision IlCilmL N/A 3E-17 IE-17 IE-16 MDC"CiirnL N/A 5E-tS 2E-IS 5E-17 MDC"CilrnL N/A 5E-IS 6E-IS 6E-ll MDCJ.lCilmL N/A lE-IS 6E-IS 7E-17 MDCJ.lCilmL N/A IE-17 3E-IS 7E-17 L.L.O.+ Effluent Conc.· % Ernuent J.lCilmL J.lCi/mL Concentration IE-16 9E-t4 2. I SE+OO IE-16 3E-14 7.17E-OI IE-16 9E-13 3.63E-02 2E-15 6E-13 1.6lE+OO L.L.D.+ Ernuent Conc. * % Effluent J.lCilmL pCilmL Concentration tE-t6 9E-14 1.76E+OO IE-16 3E-14 1.57E+OO IE-t6 9E-13 S.56E-02 2E-t5 6E-t3 6.7SE-OI L.L.D.+ Ernuent Cone. * % Ernuent pCi/mL pCilmL Concentration IE-16 9E·14 9.35E-OI IE-16 3E-14 9.32E-01 tE-t6 9E-13 1.46E-02 2E-t5 6E-13 I.t 3E+OO L.L.D.+ Effluent Cone.· % Effluent J.lCilmL IlCilmL Concentration IE-16 9E-14 1.4IE+OO IE-16 3E·14 l.nE-OI IE-16 9E-13 2.55E-02 2E-t5 6E-13 2.12E+OO Page 3 0122 EN:RGY c l\~lOIU\rCHI !'~ \WiW.energylab.com ~ExullHc'SItIc' 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid Cn" SO 188-672-1225 • College Sialion, n 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab to: Denison Mines USA Corp 4th Quarter BHV Air Cl l 0l 0188-001 Client Sample 10: BHV-l Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLtDES -TOTAL Lead 210 Lead 210 precision (±) Lead 210 MDe Radium 226 Radium 226 precision (±) Radium 226 MOe Thorium 230 Thorium 230 precision (±) Thorium 230 MOe Report Definitions: RL - Analyte reporting limit. QCl -Quality control limit. Result 0.262 177 1780 21 10 32.0 1.5 0.4 32 4.7 1.6 Units mg/fiUer pei/Filter pCilFilter pei/Filler pei/Filter pei/Filter pei/Filter pei/Filter pei/Filter pel/Filter pel/Filter MOC . Minimum detectable concentration Qualifiers RL 0.0003 0.2 Report Date: 02/08/11 Collection Date: 01/04/11 DateRecelved: 01/06/11 Matrix: Filter MCU QCL Method Analysis Date I By SW6020 01/19/11 18:53 1 sml SW6020 01119/11 18:53 1 sml E909.0 01126/11 08:42 / eli-cs E909.0 01/26/11 08:42 1 eli-cs E909.0 01126/11 08:42 / eli-cs E903.0 01/19/1118:30 /1rs E903.0 01119/11 18:30 1 Irs E903.0 01l19/11 18:30 /1rs E908.0 01124/11 10:03 1 dmf E908.0 01124111 10:03 1 dmf E908.0 01124/11 10:03 1 dmf MCl· Maximum contaminant tevel. NO . Not detected at the reporting limit. Page 4 of 22 EI\ERGY WVtW.energylab.com AD,,,,;,,/ ExcelftlnclJ Since 1951 Helena, MT 811-472-071 1 • Billings , MT 800-735-4489 • Casper, WY 888-235-051 5 Gillette, WY 866-686-7175 ' Rapid City, SD 888-672-1225 . College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: February 9, 2011 PROJECT: 4th Quarter BHY Air SAMPLE ID: BHV-2 QuartcrlDatc Sampled Concentration Air Volume Radionuclidc llei/mL C I 00402SS-002 "'IU S.47E-16 First Quarter 20 I 0 2JOTh 1.42E-J7 Air Volume in mLs 226Ra 4.66E-17 1.36E+ll 210Pb B.24E-IS QuartcrlDatc Sampled Concentration AirVoJumc Radionuclidc J.1Ci/mL C I 007033B-002 ~'U 3.SBE-16 Second Quarter 2010 2JOTh 6.64E-17 Air Volume in mLs 226Ra 9.90E-17 J.36E+II 210Pb 2.0IE-IS QuartcrlDate Sampled Concentration Air Volume Radionuclide "CilmL CI0100417-002 ~'U 2.9 IE-16 Third Quarter 2010 '30Th 4.4BE-17 Air Volume in mLs 226Ra S.72E-17 1.37E+ II 210Pb 1.0BE-IS QuarterlDate Sampled Concentration Radionuclide Air Volume "CilmL CIIOIOI8B-002 nacU S.73E-16 Fourth Quarter 20 I 0 "''Th 7.24E-17 Air Volume in mL" 226Ra 6.76E-17 J.3BE+II 210Pb J.3SE-14 +LLD's arc from Reg. Guide 4.14 *Efnuenl Concentration from the NEW 10 CFR Pari 20· Appendix B· Table 2 Year for Natural Uranium Year for Thorium·230 Week for Radium·226 Day for Lcad·210 Counling Precision MDCJlCi/mL J.lCilmL N/A N/A IE-J7 SE-IB 4E-IB 2E-IB BE-J7 SE-J7 Counting Precision MDC~C"mL Jlei/mL N/A N/A IE-J7 SE-IB IE-J7 6E-IB SE-17 6E-17 Counting Precision MDC"CilmL "Ci/mL N/A N/A IE-J7 BE-IB 9E-IB SE-IB 4E-17 4E-17 Counting Precision MDC~C"mL "CUmL N/A N/A IE-J7 4E-IB 6E-IB 3E-IB IE-16 7E-17 L.L.D.+ Effluent Cone. * % Efnuent JlCilmL /lei/mL Concentration IE-16 9E-14 6.07E-OI IE-16 3E-14 4.72E-02 IE-16 9E-13 S.IBE-03 2E-IS 6E-13 1.37E+OO L.L.D.+ Efnuent Cone. * % Effluent /lCilmL JlCilmL Concentration IE-16 9E-14 3.97E-OI IE-16 3E-14 2.2IE-OI IE-16 9E-13 1.l0E-02 2E-IS 6E-13 3.3SE-OI L.L.D.+ Ernuent Conc.· % Ernuent ~CUmL "Ci/mL Concentration IE-16 9E-14 3.23E-OI IE-16 3E-14 1.49E-OI IE-16 9E-13 6.36E-03 2E-IS 6E-13 1.79E-O I L.L.D.+ Ernuent Conc.· % Ernuent "CilmL "CUmL Concentration IE-16 9E-14 6.37E-OI IE-16 3E-14 HIE-OI IE-16 9E-13 7.5IE-03 2E-IS 6E-13 2.26E+OO Page 5 of 22 EN:RGY • I'IHOfU\rOI~ILS VNrN.energylab.com AllllybfExu/lHt,$IIu 1m Helena, NT 877·472·0711 • Billings, MT 800·135·4489 . Casper, WY 888·235·0515 Gillette, WY 866-186·7175 • Rapid City, SO 888·672·1225 • College Sialion, 1X 888·690·2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 4th Quarter BHV Air Lab 10: Cll 01 0188·002 Client Sample 10: BHV·2 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES · TOTAL Lead 210 Lead 210 precision (±) Lead 210 MDe Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±l Thorium 230 MOC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 0.117 78.9 1860 20 9.2 9.3 0.8 0.4 10 1.7 0.50 Units mg/filler pCi/Filter pCi/Filler pCi/Filter pCilFilter pCi/Filter pCI/Filter pCI/Filter pCi/Filter pCi/Filter pCi/Filter MOC -Minimum detectable concentration Qualifiers RL 0.0003 0.2 Report Dale: 02/08/11 Collection Date: 01 /04/1 1 DateReceived: 01/06/1 1 Matrix: Filter MCU QCL Method Analysis Date I By SW6020 01/19/1119:14 /sml SW6020 01/19/1119:14/sml E909.0 01i26/1115:16/eli-cs E909.0 01126/11 15:16 1 eli-cs E909.0 01/26/1115:16 /eli-cs E903.0 01119/11 22:28/ Irs E903.0 01119/11 22:28 / Irs E903.0 01/19/11 22:28 / Irs E908.0 01 /24/11 10:03 1 dmf E908.0 01/24/11 10:03 / dmf E908.0 01/24/11 10:03/ dmf MCL -Maximum conlaminanllevel. ND -Not detected at the reporting limit. Page 6 of 22 www.energylab.com _1tt/cII E.rcellence Since 1952 EN:RGY Helena, MT 817-472-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY B66-686-1115 . R.pid City, SO 888-672-1225 ' College SI.lion, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: February 9, 201 1 PROJECT: 4th Quarter BHV Air SAMPLE 10, BHV-4 QuarterlDale Sampled Concentration Radionuclide Air Volume ",Ci/mL C10040255-003 ~'U 6.0IE-15 First Quarter 2010 "''rh 1.26E-16 Air Volume in mLs 226Ra 1.34E-16 1.36E+11 210Pb 1.19E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume !lCi/mL C10070338-003 nllU 2.33E-15 Second Quarter 20 I 0 "''rh 7.29E-16 Air Volume in mLs 226Ra 2.66E-16 1.35E+1I 210Pb 3.27E-15 QuarterlDate Sampled Concentration Air Volume Radionuclide ",Ci/mL CI0100417-003 nllU 4.77E-15 Third Quarter 2010 "''rh 1.80E-15 Air Volume in mLs 226Ra 8.23E-16 1.16E+11 210Pb 5.I IE-15 QuarterlDate Sampled Concentration Radionuclide Air Volume !lCi/mL C11010188-003 ~'U 3.93E-15 Fourth Quarter 2010 "oTh 3.90E-16 Air Volume in mLs 226Ra 2.56E-16 1.37E+11 210Pb 1.l 3E-14 +LLD's are from Reg. Guide4.14 Counting Precision !lCi/mL N/A 2E-17 6E-18 IE-16 Counting Precision ",Ci/mL N/A 7E-17 2E-17 6E-17 Counting Precision !lCi/mL N/A 3E-16 5E-17 8E-17 Counting Precision !lCilmL N/A 9E-17 IE-17 IE-16 ·Ernuenl Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-2 10 MDC~CUmL N/A 4E-18 2E-18 5E-17 MDC~CUmL N/A 5E-1 8 6E-18 6E-17 MDC!lCi/mL N/A IE-17 IE-17 5E-17 MDC~CUmL N/A 6E-17 3E-18 7E-17 L.L.D.+ Effluent Cone.· % Effluent !lCi/mL !lCi/mL Concentration IE-16 9E-14 6.67E+00 IE-16 3E-14 4.19E-01 IE-16 9E-13 1.49E-02 2E-15 6E-13 1.99E+00 L.L.D.+ Effluent Cone.· % Effluent ",Ci/mL !lCi/mL Concentration IE-16 9E-14 2.59E+00 IE-16 3E-14 2.43E+00 IE-16 9E-13 2.96E-02 2E-15 6E-13 5.45E-01 L.L.D.+ Effluent Cone.· % Effluent !lCi/mL !lCi/mL Concentration IE-16 9E-14 5.30E+00 IE-16 3E-14 6.0IE+00 IE-16 9E-13 9.14E-02 2E-15 6E-13 8.52E-01 L.L.D: Effluent Cone.· % Effluent ",Ci/mL !lCi/mL Concentration IE-16 9E-14 4.37E+00 IE-16 3E-14 1.30E+00 IE-16 9E-13 2.84E-02 2E-15 6E-13 1.89E+00 Page 7 of 22 EI\ERGY 1\1 )<J!iAI ()I~1l " IWIW.energylab.com AlulytJaf bulllnct •• 1m H,lena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gill,tt" WY 866-686-7175 • Rapid Crrl, SO 888-672-1225 • ColI.g. Station, IX 888-690-221 8 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 4th Quarter BHV Air Lab 10: Cll 01 0188-003 Client Sample 10: BHV-4 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 preCision (±) Radium 226 MDe Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 0.795 538 1550 18 9.1 35.1 1.6 0.4 53 12 7.6 Units mglfilter pel/Filter pel/Filter pei/Filler pel/Filler pel/Filter pCifFilter pel/Filter pei/Filter pei/Filler pel/Filter MOC -Minimum detectable concentration Qualifiers RL 0.0003 0.2 Report Date: 02/08/11 Collection Date: 01 /04 /11 DateReceived: 01 /06 /11 Matrix: Filter MCU QCL Method Analysis Date J By SW6020 01l19/1119:18 /sml SW6020 01l1911 119:18 /sml E909.0 01/26/11 17:271 eli-cs E909.0 01126111 17:271 eli-cs E909.0 01126111 17:27 1 eli-cs E903.0 01119111 22:28/1rs E903.0 01119/11 22:2811rs E903.0 01119111 22:28/1rs E908.0 01124111 10:031 dmf E908.0 0112411 1 10:03 1 dmf E908.0 01124111 10:03 1 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 8 of 22 EN:RGY YM¥.energylab.com bl",fcal Excel/ence Since 1951 Helena. MT 87).472-0711 • Billings. MT 800-735-4489 • Casper. WY 888-135-0515 Gillelte. WY 866-686-7175 ' R.p id Cily. SO 888-672-1125 ' College SI.lion. TX 888-690-2118 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: February 9, 2011 PROJECf: 4th Quarter OHV Air SAMPLE 10: BHV-5 QuartcrlDatc Sampled Concentration Radionuclidc Air Volume J.1Ci/mL C I 0040255·004 nllU 4.7SE-15 Firsl Quarter 20 I 0 "'Th 3.73E-16 Air Volume in mls 226Ra 4.19E-16 1.36E+11 210Pb L30E-14 Quarterillatc Sampled Concentration Radionuclide Air Volume ",Ci/mL C 1007033S-004 ~u 4.3SE-IS Second Quarter 20 1 0 "'Th 7.84E-16 Air Volume in mls 226Ra LOSE-IS 1.36E+ll 2lOPb 4.40E-IS QuarterlDate Sampled Concentration Air Volume Radionuclide ,",CilmL C10100417-004 U'U 3.57E-IS Third Quarter 20 I 0 "''Th 1.14E-15 Air Volume in mLs 226Ra 7.97E-16 L03E+ II 2lOPb 3.7SE-15 QuarterlDate Sampled Concentration Radionuclide Air Volume J,lCifmL CI IOIOISS-004 U'U S.52E-IS Fourth Quarter 20 I 0 "''Th I.4SE-IS Air Volume in mLs 226Ra 1.29E-IS 1.32E+11 210Pb L33E-14 +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 eFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lcad-21O Counting Precision MDCJ.lCi/mL ,...Ci/mL N/A N/A 4E-17 6E-IS IE-17 2E-18 IE-16 SE-17 Counting Precision MDCjJCi/mL ... CUmL N/A N/A 7E-17 7E-IS 4E-17 6E-18 7E-17 6E-17 Counting Precision MDCJ.1CilmL jJCilmL N/A N/A 2E-16 2E-17 3E-17 SE-IS 7E-17 6E-17 Counting Precision MDC~CUmL J,lCifrnL N/A N/A 2E-16 3E-17 2E-17 3E-IS IE-16 7E-17 L.L.D.+ Effluent Cone. * % Effluent J.1CUmL J.1Ci/mL Concentration IE·16 9E·14 5.3 I E+OO IE-16 3E-14 1.24E+OD IE-16 9E-13 4.66E-02 2E-IS 6E-13 2.17E+OO L.L.D.+ Effluent Cone. * % Effluent J-lCilmL ",ei/mL Concentration IE-16 9E-14 4.83E+00 IE-16 3E-14 2.6IE+00 IE-16 9E-13 1.16E-01 2E-IS 6E-13 7.33E-01 L.L.D.+ Ernuent Cone. * % Effluent jJCi/mL JJCilmL Concentration IE-16 9E-14 3.97E+OO IE-16 3E-14 3.81E+OO IE-16 9E-13 S.S6E-02 2E-IS 6E-13 6.30E-01 L.L.D: Ernuent Cone. * % Ernuent ... CilmL J,lCifmL Concentration IE-16 9E-14 9.47E+00 IE-16 3E-14 4.84E+OO IE-16 9E-13 L44E-01 2E-IS 6E-13 2.22E+OO Page 9 of 22 EN:RGY /I.!,Ofl/l.! OI~!L5 www.energylab.tom AIIIIytJuI Exufllllc. SiJIc. 1151 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-186-7175 • Rapid City, SO 888-672-1225 • Colleg' Slation, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Cllenl: Projecl: Denison Mines USA Corp 4th Quarter BHV Air Lab 10: Cl I 01 01 88-004 Client Sample 10: BHV-5 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL l ead 210 l ead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDe Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: Rl . Analyte reporting limil. QCl . Quality control limit. Result 1.67 1130 1760 19 9.2 171 3.3 0.4 192 22 3.S Units mglfilter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter MDC . Minimum detectable concentration Qualifiers RL 0.0003 0.2 Report Date: 02/08/1 I Collection Date: 01104/1 I DateRecelved: 01 106/1 I Matrix: Filter MCU QCL Method Analysis Date / By SW6020 01 /19/11 19:22 1 sml SW6020 01119/11 19:22 1 sml E909.0 01 /26/11 19:39 / eli·cs E909.0 01126/11 19:391 eli-cs E909.0 01/26/11 19:39 / eli·cs E903.0 01 119/11 22:2S/lrs E903.0 01119/11 22:2S/lrs E903.0 01119/11 22:2S/lrs E90S.0 01124/11 10:03 1 dml E90S.0 01/24/1110:03 /dmf E90S.0 01 /24/11 10:03 1 dml MCl· Maximum contaminant level. ND . Not detected at the reporting limit. Page 10 of 22 EN:RGY www.energylab.com AlII"'ic~f Exc~flenc! Sinc, 1952 Helena, MI 817-471-0711 • Billings, MI 800-735-4489 ' Casper, WY 888-135-0515 Gilletle, WY 866-686-7175 . Rapid Cily, SO 888-671-1115 . College Sialion, IX 888-690-1118 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: February 9, 2011 PROJECT: 4th Quarter BHV Air SAMPLE ID: BHV-6 QuarterlDate Sampled Concentration Air Volume Radionuclide /lei/mL C1D0402SS-00S nalU 9.63E-IS First Quarter 2010 '''Th 1.82E-16 Air Volume in mu 2uRa 2.06E-16 1.36E+11 210Pb t.37E-14 QuarterlDate Sampled Concentration Air Volume Radionuclide J.lCi/mL C I 0070338-005 nalU 3.62E-IS Second Quarter 20 I 0 '''Th 3.94E-16 Air Volume in mLs 226Ra 4.89E-16 1.35E+1 1 2lOPb 4.30E-IS QuarterlDate Sampled Concentration Air Volume Radionuclide J.lCi/mL CI0100417-DOS U'U S.42E-IS Third Quarter 2010 '''Th 1.08E-IS Air Volume in mLs 126Ra S.6SE-16 I.03E+ II 210Pb 3.9SE-IS Counting Precision ",CilmL N/A 2E-17 7E-18 IE-16 Counting Precision JlCilmL N/A 4E-17 2E-17 7E-17 Counting Precision J.lCi/mL N/A 2E-16 3E-17 SE-17 QuarterlDate Sampled Concentration Counting Air Volume Radionuclide J.lCi/mL C IIOIO IBB-DOS nalU 1.24E-14 Fourth Quarter 2010 '''Th I.2IE-IS Air Volume in mLs 126Ra LODE-IS 1.1 4E+ II 210Pb I.S3E-14 +LLD's are from Reg. Guide 4.14 *Efnuenl Concentralion from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Nalural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 Precision ~CihnL N/A IE-16 2E-17 2E-16 MDC~CUmL N/A 4E-18 2E-18 SE-17 MDC/lCilmL N/A SE-18 SE-18 6E-17 MDC .... Ci/mL N/A 2E-17 6E-18 6E-17 MDC~CUmL N/A 3E-17 3E-IS 8E-17 L.L.D.+ Ernuent Cone. * % Ernuent ",Ci/mL IlCilmL Concentration IE-16 9E-14 1.07E+01 IE-16 3E-14 6.07E-01 IE-16 9E-13 2.29E-02 2E-IS 6E-13 2.29E+OO L.L.D.+ Ernucnt Cone. * % Ernucnt ,..CilmL JlCifmL Concentration IE-16 9E-14 4.02E+OO IE-16 3E-14 1.3IE+OO IE-16 9E-13 S.43E-02 2E-IS 6E-13 7.17E-01 L.L.D.+ Effluent Cone. * % Effluent .... CilmL .... CilmL Concentration IE-16 9E-14 6.02E+00 IE-16 3E-14 3.6 I E+OO IE-16 9E-13 6.3 I E-02 2E-IS 6E-13 6.63E-01 L.L.D! Effluent Cone, * % Effluent ~CilmL .... CilmL Concentration IE-16 9E-14 1.38E+OI IE-16 3E-14 4.02E+00 IE-16 9E-13 1.l2E-OI 2E-IS 6E-13 2.54E+OO Page 11 of 22 EN:RGY -u O[if\l( 1'1" www.energylab.com AIu/ftkM ExuIIIOcf Si«I '151 H,lena, MT 871-412-11111 • Billings, MT 800-135-4489 • C"per, WY 888-235-0515 Gillette, WY 866-&86-1115 · Rapid City, SD 888-672-1225 • Colleg. Stallon, TJl88S-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 4th Quarter BHV Air Cll0l0188-00S Client Sample 10 : BHV-6 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MOe Thorium 230 Thorium 230 precision (±) Thorium 230 MOe Report Definitions: RL -AnaJyte reporting limit. QCL . Quality control limit. Result 2.09 1420 1740 19 9.1 115 2.7 0.4 138 16 2.9 Units mg/fiUer pel/Filler pei/Filler pCilFilter pei/Filler pei/Filter pei/Filter pCilFiller pei/Filler pel/Filter pel/Filter MDC -Minimum detectable concentration Qualifiers RL 0.0003 0.2 Report Date: 02/08/11 Collection Date: 01/04/11 DateRecelved: 01/06111 Matrix: Filter MCW QCL Method Analysis Date I By SW6020 01119/11 19:261 smt SW6020 01/19/11 19:26 1 smt E909.0 01126/11 21 :50 I eli-cs E909.0 01126/1 1 21 :50 I eli-cs E909.0 01126/11 21 :50 I eH-es E903.0 01 119/11 22:2811rs E903.0 01 119/11 22:2811rs E903.0 01 /19/11 22:2811rs E908.0 01 124/11 10:24 1 dmf E908.0 01124111 10:24 1 dmf E908.0 01124111 10:24 1 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 12 of 22 EN:RGY www.energylab.com mlTtiell Excellence Since 1952 Helena, MT 8JJ-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillelte, WY 866-686-7175 • Rapid Cily, SO 888-672-1225 • C,lIege Slali,n, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: February 9, 2011 PROJECT: 4th Quarter BHV Air SAMPLE 10: Blank QuartcrlDatc Sampled Radionuclidc Concentration Air Volume J.lCi/mL CIOO402SS-006 nalU 1.67E-17 First Quarter 201 0 "'Th -3.03E-18 Air Volume in mls 2uRa 1.48E-18 1.36E+ II 2lOPb 3.S0E-17 Counting Precision J.lCi/mL N/A 4E-18 IE-18 3E-17 , , Note ThiS sample uses 136 000 000 L of air volume for comparison purposes QuartcrIDatc Sampled Concentration Counting Air Volume Radionuclidc ",CUmL Precision !l ei/mL CI()()70338-006 ~U 2.7IE-17 N/A Second Quarter 20 I 0 "'Th -2.63E-19 SE-18 Air Volume in mLs 226Ra 9.74E-18 4E-18 1.36E+l1 210Pb 7.47E-18 3E-17 , , Note ThIS sample uses 136 000 000 L of air volume for comparison purposes QuartcrlDatc Sampled Concentration Counting Air Volume Radionuclide ~CilmL Precision J.lCilmL CIOIOO417-006 '·u 9.0IE-18 N/A Third Quarter 20 I 0 "'Th -1.63E-18 7E-18 Air Volume in mLs lURa 1.27E-18 4E-18 1.36E+II 210Pb -2.26E-17 3E-17 .. , , Note 1 hiS sltmple uses 136 000 000 L of air volume for comparison purposes QuarterlDate Sampled Concentration Counting Air Volume Radionuclide J.lCilmL Precision J.lCilmL C11010188-006 natu 9.3SE-18 N/A Fourth Quarter 20 I 0 "''Th -6.17E-19 2E-18 Air Volume in mLs 226Ra -6.8SE-19 2E-18 1.36E+ II 210Pb S.87E-18 4E-17 .. Note. 1 hiS sample uses 136,000,000 L of air volume for comparison purposes. +LLD's are from Reg. Guide4.14 *Erfluent Concentration from the NEW 10 CFR Part 20 -Appendix: B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lcad-2 1 0 MDC~CUmL N/A SE-18 2E-18 SE-l7 MDC~CUmL N/A 6E-18 SE-18 6E-17 MDCpCilmL N/A IE-l7 7E-18 4E-17 MDCJ.lCilmL N/A 2E-18 3E-18 7E-17 L.L.D.+ Ernuent Cone. * % Effluent ~CUmL IlCi/mL Concentration IE-16 9E-14 1.86E-02 IE-16 3E-14 -1.0IE-02 IE-16 9E-13 I.64E-04 2E-IS 6E-13 S.83E-03 L.L.D.+ Ernucnt Cone,· % Effluent jJCilmL IlCilmL Concentration IE-16 9E-14 3.02E-02 IE-16 3E-14 -8.7SE-04 IE-16 9E-13 1.08E-03 2E-IS 6E-13 1.24E-03 L.L.D.+ Efnuent Cone.· % Efnuent J.lCi/mL J.lCilmL Concentration IE-16 9E-14 1.00E-02 IE-16 3E-14 -S.44E-03 IE-16 9E-13 1.4 I E-04 2E-IS 6E-13 -3.76E-03 L.L.D.+ Efnuent Cone.· % Efnuent J.lCilmL J.lCilmL Concentration IE-16 9E-14 I.04E-02 IE-16 3E-14 -2.06E-03 IE-16 9E-13 -7.6IE-OS 2E-IS 6E-13 9.78E-04 Page 13 0122 EN:RGY ,'\1 OIU'd( 1111', YfoNW.energylab.com AIIIJtitM Exullfou SJIu IIS1 Helena, MT 877-472-0711 • Billing', MT 800-731-4489 • Cuper, WI 888-235-0515 Gillette, WI 866-186-7175 • Rapid City, SO 888-672-1225 • College SI,'ion, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Clienl: Project: lab 10: Denison Mines USA Corp 41h Quarler BHV Air Cll0l0188-006 Client Sample 10: Blank Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) Lead 210 MDe Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0019 1.3 0.80 5.5 9.2 -0.09 0.2 0.4 -0.08 0.25 0.32 Units mg/filter pCI/Filler pCi/Filler pCi/Filter pCilFiller pCilFiller pCilFiller pCilFilter pCi/Filter pCiJFilter pCiJFiller MOC -Minimum detectable concentration Report Date: 02/08/11 Collection Date: 01 /04/11 DateRecelved: 01 /06/11 Matrix: Filter MCU Qualifiers RL QCL Method Analysis Date 1 By 0.0003 SW6020 01 /19/11 19:30 / sml 0.2 SW6020 01 /19/11 19:30/ sml U E909.0 01 /27111 00:02 1 eli-cs E909.0 01 /27/11 00:02 / eli-cs E909.0 01 /27/11 00:02 / eli-cs U E903.0 01 /19/1122:28 /lrs E903.0 01 /19/11 22:2811rs E903.0 01119/11 22:2811rs U E908.0 01124/11 10:03 / dmf E908.0 01124/11 10:03 / dmf E908.0 01124/11 10:03 / dmf MCl -Maximum contaminant ievel. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 140122 EN:RGY ,\! OUi'>.! "1<11 " www.enefgylab.com AnIIytJuI ExullHc. SlIt. tez Helena, MT 877-412-l1111 • Billin!., MT 80D-135-4489 • Casper, WY 888-235-0515 Gill.tt., WY 866-586-1115 • Rapid Clly, SO 888-612-1225 • Coli.!. Slation, TJ( 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter BHV Air Analyle Count Result Units Method: E903.0 Sample 10: Cll010238-001AMS Radium 226 Sample 10: Cll010238-001AMSO Radium 226 Sample 10: LCS-28735 Radium 226 Sample 10: MB-28735 Radium 226 Radium 226 precision (±) Radium 226 MOe Qualifiers: RL -Analyle reporting limit. Sample Matrix Spike 44.5 pel/Filter Sample Matrix Spike Duplicate 42.9 pel/Filter Laboratory Control Sample 13.3 pei/Filter 3 Method Blank -0.2 pei/Filter 0.09 pei/Filter 0.2 pei/Filter MDe • Minimum detectable concentration Report Date: 02/08/11 Work Order: Cl 1 01 0188 RL %REC Low Limit High Limit RPO RPOLlmlt Qual Run: BERTHOLD 770-Ul0113B 111 70 130 Run: BERTHOLD 770-Ul0113B 107 70 130 3.5 Run: BERTHOLD 770-1_110113B 112 70 130 Run: BERTHOLD 770-1_110113B NO -Not detected althe reporting limil. U -Not detected al minimum detectable concentration Batch: R142010 01 /19111 14:28 01119111 18:30 20.8 0111911118:30 0111911118:30 U Page 15 of 22 EN:RGY ,\1 ,OIIAI (JI.j11 <J www.energyillb.com AMIytk6IEx.ulltiJt.SIJIu 1m Hel"" lIlT 877-472-0711 • Billing., MT 800-735-4489 • Cosper, WY 888-235-0515 Gillette, WI 866-186-7175 • Rapid City, SD 888-672-1225 • College SI,lioo, IX 888-680-2218 Client: Denison Mines USA Corp Project: 41h Quarler BHV Air QA/QC Summary Report Prepared by Casper, WY Branch Report Date: 02/08/1 I Work Order: CI IOIOl88 Analyte Count Result Units RL %REC Low Limit High limit RPD RPOLimit Qual Method: E908.0 Sample 10: CIIOIOI88-00IAMS Thorium 230 Sample 10: CIIOIOI88-001AMSO Thorium 230 Sample 10: LCS-28739 Thorium 230 Sample 10: MB-2B739 Thorium 230 Thorium 230 precision (±) Thorium 230 MOe Qualifiers: RL -Analyte reporting limit. 3 MOe -Minimum detectable concentration Sample Matrix Spike 248 pei/Filter Sample Matrix Spike Duplicate 228 pel/Filler Laboratory Control Sample 11 .5 pei/Filler Method Blank -0.2 pei/Filter 0.08 pel/Filter 0.1 pei/Filter Balch: 28739 Run: EGG-ORTEC_ll0120A 01124/11 10:03 111 70 130 Run: EGG-ORTEC_ll0120A 01124/11 10:03 101 70 130 8.4 30.2 Run: EGG-ORTEC_ll0120A 01/24/11 10:03 120 70 130 Run: EGG-ORTEC_ll0120A 01/24/1110:03 U NO · Not detected at the reporting limit. U -Not detected at minimum delectable concentration Page 160122 EN:RGY IWIW.energylab.com Helena, MT 817-472-0711 • Bilnng., MT 800-735-4489 ' Casper, WY 818-235-0515 GiII.rt., WY 866-186-7175 ' Rapid CHy, SO 888-672-1225 ' College St.tion, TX 888-610-2218 ;\1 O!,/\I( UI " AMIftJcM ExullHc. st.u ,m QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 4th Quarter BHV Air Analyte Count Result Units Method: E909.0 Sample 10: Cll0l0188-001AMSO Lead 210 Sample 10: Cll0l0188-001AMS Lead 210 Sample 10: LCS-13081 Lead 210 Sample 10: MB-13081 Lead 210 Lead 210 precision (±) Lead 210 MDe Qualifiers: RL -Anaryte reporting rimit. 3 MDe -Minimum detectable concentration Sample Matrix Spike Duplicate 2930 pei/Filler Sample Matrix Spike 3040 pCi/Filter Laboratory Control Sample 349 pCi/Filter Method Blank 5 pei/Filter 6 pei/Filter 9 pei/Filter Report Date: 02/08/11 Work Order: Cll0l0188 RL %REC Low Limit High Limit Run: SUB-T38663 106 70 130 Run: SUB-T38663 117 70 130 Run: SUB-T38663 96 70 130 Run: SUB-T38663 ND -Not detected at the reporting limit. RPD RPDLimit Qual 3.7 Balch: T_13081 01/26111 13:05 13 01126/11 10:53 01126/11 06:30 01 /26ft 1 02:07 U U -Not detected at minimum detectable concentration Page 17 of 22 EN:RGY www.energylab.com Helen" MT 817-472-0711 • Billing" MT 800-735-4489 • Cuper, W'l 888-235-0515 Gillette, W'l 866-186-7175 • Rapid Cny, SO 888-672-1225 • College St.tion, IX 888-691l-2218 '"\\ OIUd( 1,,11 '. AIuIftIuI lxuflMJcf SiIIc. tID Client: Denison Mines USA Corp Project: 4th Quarter SHV Air QA/QC Summary Report Prepared by Casper, WY Branch Report Date: 02/08/11 Work Order: Cl l0l 0188 Analyte Count Result Units RL %REC Low Limit High limit APD RPOLimit Qual Method: SW6020 Sample 10: MB-28739 Uranium Sample 10: LCS2-28739 Uranium Sample 10: Cl1010188-006AMS Uranium Sample 10: Cll0l0188-006AMSO Uranium Qualifiers: RL -Analyle reporting limit. MOe -Minimum detectable concentration Method Blank 6E-OS mglfiller Laboratory Control Sample 0.0998 mg/fitter Sample Matrix Spike 0.0577 mg/filler Sample Matrix Spike Duplicate 6E-05 0.00030 0.00030 0.0572 mg/filler 0.00030 Run: ICPMS2-C_"0119A Run: ICPMS2-C_"0119A 100 85 115 Run: ICPMS2-C_"0119A 112 75 125 Run: ICPMS2-C_"0119A 11 1 75 125 NO -Not detected althe reporting limit. 0.7 Batch: 28739 0111911 1 18:41 01119111 18:45 01119111 19:34 01119111 19:38 20 Page 18 of 22 EI\ERGY "IJ~'1 ,'!ClIl ~ WWIII.energylab.com AI&JIrtjaI CxWItIIct st.u ,m Helena, MT 877-472-0111 • Billings, NT 800-735-4489 • Cuper, WY 888-235-0515 Gillette, WI 866·688·7175 • Rapid City, SO IIB·&72·1225 • College SI,tlon, IX 88B·6BO·221 B Workorder Receipt Checklist Denison Mines USA Corp C11010188 Login completed by: Halley Ackerman Reviewed by: BL2000ltedwards Reviewed Date: 1/8/201 1 Shipping container/cooler in good condition? Custody seats inlact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sam pie labels? Samples in proper containerlbottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding lime? ContainerfTemp Blank temperature: Waler -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Ves 0 Ves 0 Ves 0 Ves 0 Ves 0 Ves 0 Ves 0 Ves 0 Ves 0 Ves 0 ·c Ves 0 Ves 0 Date Received: 1/6/201 1 Received by: ha No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 NoD Carrier name: Next Day Air Not Present 0 Not Present 0 Not Present 0" No VOA vials submitted 0" Not Applicable 0" Page 19 0122 /U1;i!i' Chain of Custody and Analytical Request Record Page -.L of L- 'l·m_Olk.udi ' PLEASE PRINT Provide as much information as ossible. Compa~e: Project Name, PWS, Permrt, Etc. Sample Origin EPNState Compliance: J/<""5C"} fJ1,~€S. 'fit (2~ r< P ..i3it...v A;~ State: r..<.j' Yes 0 No 0 I-Report Mail Address: p.o .-&~ 8'01 .. Phone/Fax: Email: .: (Plea,/)print) ElartA0:J 1.A"f <r'lSI( 73 .... #I~r- Invoice Address: Purchase Order: e Order: ~Sa~ ~~~ Special Report/Formats: ;: I &ll&\ill, \7@1J@ OO@:®{)iJ~ Dow D POTWIWWTP D State: ___ _ D Other: ___ _ o to ~o V)..t:= ~aJ:201 Q) "i9>g iQm D EOO/EOT(Electronic Data) §~~ ~ ~ F t· u>ooe orma . _c«(J)~ml32 D LEVEL IV ~ ~lg C§ ::J 11)-3"ii ~ zo.."'",.Ig'Cl \ .~ E >1 """" ~ ~ D NELAC E0=I" ' ~ SAMPLE IDENTIFICATION Collection MATRIX 1....-CSiS Name. Location, Interval, etc. Time \- 5/11/-/ I '~I I ~-.4 1/1/111 1 "ISIw-:J I I I ) I II/!LJL i'/!,}f1l-1./ I I I I 1/1/1/1/ '~i3f1Y-;;-I I 1 I l 1/1/1/11 "!5IfV-.h I I I I I r/l/I'/1/ "Lkn/{. -l,o~1 IIS-iJ VI/II JL 7 8 • " ,Custody hd8r,~~f!!] Record MUST bel----- D·'tS.2t?//£~~1 Sign~ Sample Return to Client: Lab , u, Recet""Eld ""bY{iijnt): KIIIC8IV:<i by abO Cl UJ I () <{ I-l-<{ UJ UJ (/) ~ t:. '0 e " e ro e :; t- 'E '" '0 c g; .. R U 5 H JateITime. Contact ELI prior to RUSH sample submittal ::>nlppea Dy: ol.rlOjs): for charges and scheduling -See Instruction Page C~ Comments: I RoceipUemp t-l 11=1-0 c On"." Y 0 50 Custody Seal On Bottle Y N On Cooler C!> N ' ,ntact 6 N Signature (\)0. N Match V 1'= ~ ~ -I ~1\l'10~ I"'] Signature: Signature: l:k.\ \ __ ~ llk-;I~na;:'. In certain circumstances , samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. _All sub-contract data will be clearly notated on your analytical report. Week 2 ) 4 5 6 7 8 9 I. II 12 Week • 1 2 3 4 5 6 7 8 9 to 11 t2 13 Week • 1 2 3 4 5 6 7 8 9 to 11 t2 t3 Week 2 3 4 5 6 7 8 9 10 11 12 Period: October 4, 20tO through January 3, 2011 (4th Quaner 2010) SHV·1 on stream % Filter 815J751 8153743 8153736 81537)0 8153724 8153721 8400799 8400793 8400787 815371 3 8400781 Start II-Oct-IO IS·Oct·IO 25-Oct-1O Ol-Nov-ID OS-Nov·lQ IS-Nov-ID 22-Nov-1O 19-Nuv-IQ Q6.Dec·lO I3-Dee-\0 20-Dec-1O 27-Dec-1O BHV-2 on stream % Filter Start Number Dale 8153756 04-OcI-l0 8153750 It·Oct·IO 8153742 16-Oct-l0 8153737 25-0ct-IO 8153731 01-Nov-la 8153725 08·Nov-tO 8153720 15-Nov·l0 8400796 22-Nov-l0 8400792 29·Nov-l0 8400786 06-Dec·10 8153712 f3·0ec-l0 8400780 20-Dec-l0 8400774 27-Dec·10 Totals 91 BHV-4 on stream % Filter Start Number Dale 8153755 04-0ct-l 0 8153749 If-Ocl·l 0 8153744 l8-Oct-l0 8153738 25-Oct-l0 8153732 01 -Nov-l0 8153726 OB-Nov'10 8153719 15-Nov-l0 8400797 22-Nov·l0 8400791 29-Nov-l0 8400785 06-Dec-tO 8153714 l3-Dec-l0 8400779 20-Dec-l0 8400773 27-0ec-l0 Totals 91 BHV-5 ot'! stream % Filtor 8153748 8153745 8153739 8153733 8153727 8153718 8400796 8400790 8400784 8153715 8400778 Slart 11-0cl-10 IS·Ocl·l0 25-0ct-l0 01 -Nov-l0 06-Nov·10 lS-Nov-l0 22-Nov-l0 29-Nov-l0 06·0ac-l0 13·Dec-10 20-Deo·l0 102.2% Stop I IS-Oct-IO 2.'5-Oct-1O I-Nov-IO S-Nov-lO IS-Nov-to 22-Nov-IO 29-Nov.JO 6·Dec-IQ B-Dec-IO 20-Dee-IO 21-Dec-1O 3-Jan-1 100.9% Stop Dale I I-Oct-tO 18·0ct-10 25-0ct-l0 Ol-Nov-IO 08-Nov·10 IS-Nov·l0 22-Nov-l0 29-Nov-l0 06·0ec-l0 13-Dec·l0 20·0ec-l0 27-0ec-l0 03·Jan-l t 2164.0 100.4% Stop Dale l'-Oct-10 18-act-l0 25·Oct-l0 01-Nov-tO OS-Nov-1D IS-Nov-tO 22·Nov-l0 29-Nov-l0 06·Dec-tO 13-Dec-tO 20-Dec-tO 27·Dec·l0 03-Jan·l1 2184.0 97.0% Stop 4.6114 4.6300 4.6042 4.5985 4.5675 4.6649 4.3964 4.4149 4.3400 4 . .'56.'50 4.3770 Gross 4.6558 4.8884 4.6982 4.71 17 4.8941 4.6425 4.6875 4.3874 4.5169 4.5942 4.9186 4.4026 4.4131 4.64702 Gross 4.6277 4.5621 4.5379 4.6317 4.5852 4.5446 4.6159 4.3800 4.3681 4.4135 4.6373 4.4345 4.3400 4.51373 4.4907 4.5 162 4.4847 4.4963 4.4975 4.5022 4.1181 4.3232 4.2748 4.4828 4.3017 Tare 4.4929 4.5064 4.4956 4.5124 4.4974 4.4973 4.4761 4.2713 4.3057 4.3216 4.4548 4.3059 4.3097 4.41919 Tare 4.4906 4.5019 4.5102 4.5080 4.4708 4.4766 4.4715 4.3246 4.2792 4.3173 4.4844 4.3133 4.3156 4.42032 18·0ct-l0 4.6539 4.4987 25-0ct-l0 4.5624 4.4620 01-Nov-l0 4.6310 4.4977 OB-Nov-10 4.6705 4.5074 15·Nov·l0 4.5668 4.4867 22-Nov-l0 4.6642 4.5013 29·Nov-10 4.4145 4.3409 06-Dec-l0 4.4680 4.3257 13·Dec-l0 4.3913 4.2829 20-000-10 4.6276 4.4863 27-000-10 4.3672 4.2623 I 0.1200 0.1138 O.1!95 0.1022 0.0700 0.1627 0.0783 0.0917 0,0652 0.0822 0.0753 Net 0.1629 0.3800 0.2024 0.1993 0.3967 0.1452 0.2114 0.1161 0.2112 0.2724 0.4638 0.0969 0.1034 0.2278 Nel 0.1371 0.0602 0.0277 0.1237 0.1144 0.0678 0.1444 0.0554 0.0889 0.0962 0.1529 0.1212 0.0244 0.0934 0.t552 0.0804 0.1333 0.1631 0.0801 0.1629 0.0736 0.1423 0.1084 0.1413 0.1049 SlOp 24652.4 24824.1 24989.1 25 158.0 25324.7 25497.5 25664.3 25833.3 25999.9 26168.7 26337.5 Stop Time 34672.0 34840.9 35013.7 35176.9 35347.1 35513.5 35686.1 35653.4 36022.5 36188.5 36358.0 36526.1 36712.9 Slop Time 10328.1 10495.0 10666.0 10830.7 11000.8 11167.4 11340.2 11507.3 11676.6 11835.5 12002.8 12170.9 12359.4 Stop 34180.7 34351.7 34516.6 34686.6 34853.1 35025.9 35192.4 35361.7 35521.2 35687.9 35856.1 Start 24483.5 24652.4 24824.1 24959.1 2!i1!i8.0 25324.7 25497.5 25664.3 251133.3 25999.9 26168.7 BHV-2 Start Time 34509. , 34672.6 34840.9 35013.7 35176.9 35347.1 35513.5 35686.1 35853.4 36022.5 36188.5 36358.0 36526.1 BHV·4 Start Time t0165.7 10328.1 10495.0 10666.0 10830.7 11000.8 11167.4 11340.2 11507.3 11676.6 11835.5 12002.8 12170.9 SHY-5 Start 34018.8 34180.7 34351.7 34516.6 34686.6 34853.1 35025.9 35192.4 35361.7 35521.2 35687.9 Total 10134.6 10302.0 9898.2 11935.8 10000.2 10366.8 10009.8 10141.8 9996.0 10125.6 10130.4 I I Total Time 9174.0 10095.6 10368.0 9793.& 10214.4 9979.& 10359.6 10036.2 10147.8 9959.4 10168.8 10086.0 11205.0 132166.4 Tolal Time 9741.0 10013.4 10259,4 98116.2 10206.6 9995.4 10368.0 10022,4 10162.2 9532.8 100]4.4 10088.4 11312.4 131622.6 Total 5479.8 9726.6 10261 .8 9891.6 10204.8 998&.8 10365.6 9993.6 10153.8 9574.8 9997.8 10092.0 Total Volume: Total 10.618,257 10.193,646 10,370,575 12.505,416 10,477,443 10,832,18] 10,459,156 10.597,082 10,359,820 10,436,792 10,441,740 4,92E+06 Loading, Per Cent 0.0114 0.0105 0.0115 0.0082 0.0067 0.0150 0.0075 0.0087 0.0063 0.0019 0.0072 95,7% 100.5% 102.2% 98.2% 118.4% 99.2% 102.8% 99.3% 100.6% 99.2% 100.5% 10(l5% Tolal Volume: 4.SSE+06 Tolal Loading, Per Cent Liters malm3 On Siream 10,102,063 0.0161 97.0% 10,577,396 0.0359 100.2% 10,862,796 0.0186 102.9% 10,261,193 0.0194 97.2% 10,701,865 0.0371 101.3% 10,456,069 0.0139 99.0% 10,824,660 0.0195 102.8% 10,486,742 0.0111 99.6% 10,603,352 0.0199 100.7% 10,321 ,888 0.0264 98.8% 10,481,320 0.0443 100.9% 10,395,975 0.0093 100.1% 11 ,549,366 0.0090 1 11 .~1o 137.624,685 0.0216 100.9% Tolal Volume: 4.B4E+06 Total Loading, Per Cent Lilers malm3 On Stream 10,067,956 0.0136 96.6% 10,491 ,273 0.0057 99.3% 10,749,013 0.0026 101.8% 10,358,002 0.0119 98.1% 10,693,693 0.0107 101.3% 10,472,414 0.0065 99.2'r .. 10,833,437 0,0133 t02,9% 10,472,322 0.0053 99.4% 10,618,398 0.0084 100.8"10 9,879,762 0.0097 94.6% 10,342,790 0.0148 99.5% 10,398,449 0.0117 100.1% 11,660,067 0.0021 112.2% 137,037,574 0.0089 100.4% Total Voll.lme: 4.67E+06 Total 5,663,729 10,190,786 10,751,527 10,363,660 10,691,807 10,465,499 10,830,929 10,442,229 10,609,621 9,923,290 10,305,065 10,402,160 loading. Per Cenl 0.0150 0.0152 0.0075 0.0129 0.0153 0.0077 0.D150 0.0070 0.0134 0.0109 0.0137 0.0101 54.4% 96.5% 101.8% 98.1% 101.2% 99.1% 102.8% 99.1% 100.7% 95.0% 99.2% 100.1% Page 1 36.5 31.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 -'6.6 -'6.4 36.4 SCFM 36.5 37.0 37.0 37.0 ]7.0 37.0 36.9 36.9 36.9 36.b 36,4 36.4 36.4 36.& SCFM 36.5 37.0 37.0 31.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.& 36.5 37.0 ]7.0 ]7.0 37.0 37.0 36.9 36.9 ]6.9 36.6 36.4 36.4 Period: October 4, 2010 through January 3,2011 (4th Quarter 2010) Pag92 SHV-6 on stream % 83.6% BHV-6 Total Volume: 4.03E+06 Week Filter Star! Slop Slop Start Total Total loading, Per Cent 36.S 2 8153747 11-Oct-l0 18-Oct-10 4.7006 4.5036 0.1970 176.2 12.6 9814.2 10,282,566 0.0192 97.4% 37,0 3 8153746 18-Oct-tO 25-0ct-l0 4.5707 4,5052 0.0655 347.2 176.2 10260.6 10,750,270 0,0061 101 .8% 37.0 4 8153740 2S-Oct-l0 01-Nov-l0 4.6320 4.5128 0.1192 512.0 347.2 9888.6 10,360,517 0.0115 98.1% 37.0 5 8153734 OI-Nov-tO 08-Nov-IO 6.6356 4,5119 2.1231 882.1 512.0 10202.4 10,689,293 0.1987 101.2% 37.0 6 8153728 08-Nov-tO t5-Nov-l0 4.5625 4.4845 0.0780 848.6 682.1 9994.2 10,471,157 0.0074 99.1% 37.0 7 8153717 IS·Nov-IO 22-Nov-IO 4.6500 4.4814 0.1686 1021.1 848,6 10348,2 10,812,748 0.0166 102.7% 36.9 8 6400795 22-Nov-l0 29-Nov·l0 4.3748 4,3010 0.0738 1188.2 t021.1 10027.2 10,477,336 0.0070 99.5% J6.9 9 8400789 29-Nov-l0 06-0ec-l0 4.4593 4.3265 0.1328 1357.5 1188.2 101.57.4 10,613,362 0.0125 100.8% 36,9 10 8400783 OS-Oec-IO la-Dec-IO 4.3943 4.3t39 0.0804 1471 .9 1357.5 6864.6 7,114,448 0.01 13 68.1% 36 .• t1 8153716 13·oec-tO 20-0ec-IO 4.5203 4.4768 0.0435 1536.5 1471.9 3874.2 3,993,267 0.0109 38.4% 36.4 12 8400777 20-Dec-IO 27-0ec-l0 4.3881 4.3223 0.0656 1636.2 1536.5 .5982.0 6,165,646 0.0107 59.3% 36.4 ALL BHV on stream % 96.8% Week Slart Slop -Ocl-l 0 4.4861 2 8153741 11-Oct-l0 18-Det-tO 4.5067 3 8153735 18-Oct·10 25-Oct-l 0 4.4000 4 8153729 25-Oct-10 01 -Nov-IO 4.4SOO 5 8153723 01·No\l-10 OS-Nov-l0 4.4755 6 6153722 08-Nov-tO 15-Nov-l0 4.4934 7 8400800 IS·Nov-IO 22-Nov-l0 4.3225 6 8400794 22-Nov-l0 29-Nov-l0 4.3040 9 8400788 29-Nov-l0 06-Dec-l0 4.3006 10 8153711 OS-Dee-tO l3·Dec·l0 4.4844 11 8400762 13-Dec-l0 20-Dec-IO 4.3276 12 8400776 20-Dec·l0 27-0ec-l0 4.2791 ATTACHMENT D AIR PARTICULATE LOADING GRAPHS AND SUPPORTING DATA 0 0 0 " >-' a a a >-' a 0 0 >-' 0 0 0 >-' 0 0 0 >-' 0 0 0 0 1/5/2009 1/26/2009 2/16/2009 3/9/2009 3/30/2009 4/20/2009 5/11/2009 6/1/2009 6/22/2009 ~ + 7/13/2009 .., '" 8/3/2009 VI I r+ -;:: Q1 >-' 8/24/2009 r+ _. + 0 9/14/2009 ::s -a '" 10/5/2009 I Q1 -;:: 10/26/2009 .., N r+ _. f 11/16/2009 n c: 12/7/2009 Q1 '" I r+ 1: 12/28/2009 tD r- + 1/18/2010 0 Q1 2/8/2010 c.. '" -. I 3/1/2010 ::s < OQ en 3/22/2010 - + 4/12/2010 3 OQ '" 5/3/2010 ...... I 3 < '" 5/24/2010 w - 6/14/2010 7/5/2010 7/26/2010 8/16/2010 9/6/2010 9/27/2010 10/18/2010 11/8/2010 11/29/2010 12/20/2010 0 0 P >-' 0 0 >-' 0 0 >-' 0 0 >-' 0 0 0 0 0 0 0 1/5/2009 1/26/2009 2/16/2009 3/9/2009 3/30/2009 4/20/2009 5/11/2009 6/1/2009 6/22/2009 7/13/2009 o:J 8/3/2009 :::t < I 8/24/2009 ..... 9/14/2009 "'tJ II) 10/5/2009 .., .... -. 10/26/2009 n s:::: t 11/16/2009 II) .... 12/7/2009 tD '" :J: r-< 12/28/2009 0 e. II) 1/18/2010 Q. 2/8/2010 :::l at! 3/1/2010 -3 3/22/2010 at! 4/12/2010 ........ 3 5/3/2010 w -5/24/2010 6/14/2010 7/5/2010 7/26/2010 8/16/2010 9/6/2010 9/27/2010 10/18/2010 11/8/2010 11/29/2010 12/20/2010 0 0 !" >-' 0 0 >-' 0 0 >-' 0 0 >-' 0 0 0 0 0 0 0 1/5/2009 1/26/2009 2/16/2009 3/9/2009 3/30/2009 4/20/2009 5/11/2009 6/1/2009 6/22/2009 7/13/2009 '" 8/3/2009 ::I: < I 8/24/2009 N 9/14/2009 "'C Qj 10/5/2009 '"l .... _. 10/26/2009 n c: + 11/16/2009 Qj .... 12/7/2009 tD OJ :l: r-< 12/28/2009 0 N Qj 1/18/2010 c.. -. 2/8/2010 ::l OQ 3/1/2010 - 3/22/2010 3 OQ 4/12/2010 ........ 3 5/3/2010 w -5/24/2010 6/14/2010 7/5/2010 7/26/2010 8/16/2010 9/6/2010 9/27/2010 10/18/2010 11/8/2010 11/29/2010 12/20/2010 0 0 0 P >-' 0 0 0 >-' 0 0 0 >-' 0 0 0 >-' 0 0 0 >-' 0 0 0 0 1/5/2009 1/26/2009 2/16/2009 3/9/2009 3/30/2009 4/20/2009 5/11/2009 6/1/2009 6/22/2009 7/13/2009 C::I 8/3/2009 ::z:: < 8/24/2009 I ~ 9/14/2009 "'C !U 10/5/2009 ~ -. 10/26/2009 n c: - + 11/16/2009 !U .... 12/7/2009 CD '" ::t: .... < 12/28/2009 0 J,. !U 1/18/2010 a. -. 2/8/2010 ::J OQ 3/1/2010 - 3/22/2010 3 OQ 4/12/2010 ........ 3 5/3/2010 w -5/24/2010 6/14/2010 7/5/2010 7/26/2010 8/16/2010 9/6/2010 9/27/2010 10/18/2010 11/8/2010 11/29/2010 12/20/2010 0 0 !=' .... 0 0 .... 0 0 .... 0 0 .... 0 0 0 0 0 0 0 1/5/2009 1/26/2009 2/16/2009 3/9/2009 3/30/2009 4/20/2009 5/11/2009 6/1/2009 6/22/2009 7/13/2009 OJ 8/3/2009 :::I: < 8/24/2009 I U1 9/14/2009 "'C III 10/5/2009 ~ -. 10/26/2009 n s:: - + 11/16/2009 III .... 12/7/2009 to '" I r--::: 12/28/2009 0 In III 1/18/2010 c.. -. 2/8/2010 ::J OQ 3/1/2010 -3 3/22/2010 OQ 4/12/2010 ...... 3 5/3/2010 IN -5/24/2010 6/14/2010 7/5/2010 7/26/2010 8/16/2010 9/6/2010 9/27/2010 10/18/2010 11/8/2010 11/29/2010 12/20/2010 0 0 p .... a a .... a 0 .... 0 0 .... 0 0 0 0 0 0 0 1/5/2009 1/26/2009 2/16/2009 3/9/2009 3/30/2009 4/20/2009 5/11/2009 6/1/2009 6/22/2009 7/13/2009 o:J 8/3/2009 :::I: < 8/24/2009 I en 9/14/2009 "'tI II) 10/5/2009 ;::l. -. 10/26/2009 n C -11/16/2009 + II) r+ 12/7/2009 tD OJ I r--;:: 12/28/2009 0 '" II) 1/18/2010 c.. 2/8/2010 :::s C1Q 3/1/2010 -3 3/22/2010 C1Q 4/12/2010 ........ 3 5/3/2010 w -5/24/2010 6/14/2010 7/5/2010 7/26/2010 8/16/2010 9/6/2010 9/27/2010 10/18/2010 11/8/2010 11/29/2010 12/20/2010 Week , , 4 , 6 7 8 9 .0 II L2 Week 2 3 4 5 6 7 8 9 10 11 12 13 Week 2 3 4 5 6 7 8 9 10 " 12 Period; July 5, 2010 through October 4, 2010 (3rd Quarter 2010) BHV-1 Oil stream % Filter 8155031 8155026 8155015 8155012 8155006 8153799 8153'193 8153784 8153778 8153772 8153769 Start 5-1u1-10 12-1ul-1O 19-Jul-1O 26-Jul-IQ 02-Aug-1O 09-Aug-IO 16-Aug-1O 23-Aug-JO JO.Aug-JO 06·Sep·lO !3·Sep-JO 20-Scp-JO BHV-2 on stream % Fitter 8155030 8155025 8155016 815501 t 8155005 8153798 8153792 8153785 8153779 8153773 8153768 Start 12-Jul-10 19-Jul-l0 26-Jul-1O 02-Aug-l0 09-Aug-l0 16-Aug-10 23-Aug-10 30-Aug-10 06-Sep-10 13-Sep-l0 20-Sep-l0 BHV-4 on stream % Filter 6155024 8155017 8155010 815S004 8153797 8153791 8153786 8153780 8153774 8153767 Start 19·Jul-l0 26-Jul-10 02-Aug-10 0~Aug-1 0 16-Au9"'0 23-Aug-l0 3O-Aug-10 06-Sep-10 13-Sep-10 2o-sep.1a 100.2% Stop Il-Jul-JO 19-Jul-l0 26-Jul-1O 2-Aug-1O g.Aug-1O 16-Aug-IO 23-Aug-IO 3O-Aug-IO 6-Sep-LO I)-'Sep-lO 20-Scp-JO 27-Sep-IO 100.0% Stop 4.6330 4.6S48 4.6658 4.6143 4.5842 4.6506 4.6067 4.6648 4.7252 4.5427 4.7300 4.5843 4.4684 4.4863 4.4842 4.4939 4.4953 4.4682 4.4309 4.4974 4.4899 4.4993 4.4992 0.1864 0.1795 0.1301 0.0903 0.1553 0.1385 0.1339 0.2278 0.0528 0.2307 0,0851 19-Jul-l0 4.9067 4.4617 0.4450 26·Jul-tO 4.7560 4.5055 0.2505 02-Aug-l0 4.7152 4.5019 0.2133 09-Aug-l0 4.6878 4.4792 0.2086 16-Aug-l0 4.6159 4.4915 0.3244 23-Aug-l0 4.8275 4.5056 0.3219 30-Aug-10 5.0157 4.4924 0.5233 OS-SSP-10 5.00n 4.4786 0.5291 13-Sep-l0 4.6156 4.4789 0.1369 20-Sep-10 4.9615 4.4748 0.4867 27-Sep-10 4.6552 4.4955 0.1597 84.7% Stop 26-Jul·10 4.8615 4.4440 0.4175 02·Aug-10 4.7460 4.5116 0.2344 09-Aug-10 4.7151 4.5039 0.2112 16-Aug-10 4.7384 4.5081 0.2303 23-Aug-l0 4.7419 4.5091 0.2328 3O-Aug-l0 4.7888 4.5037 0.2851 06-Sep-10 4.7040 4.4731 0.2309 13-Sep·l0 4.6258 4.4941 0.1317 2O-Sep-l0 4.886B . 4.4816 0.4052 27-Sep-10 4.5147 4.4810 0.0337 Stop 22305.0 22474.1 22641.7 22806.6 22998.1 23145.8 23310.8 23478.4 23761.6 23812.3 24027.9 24148.3 Stop 32494.0 32663.0 32830.4 32995.9 33187.1 33334.8 33500.7 336£7.5 338SO.0 34001.3 34216.9 34337.3 SlOp 8467.5 8654.6 8842.9 8990.6 9155.9 9323.7 9515.6 9657.3 9671.8 9993.5 BHV-1 Start 22305.0 22474.1 22641.0 22806.6 22998.1 23145.8 23310.8 23478.4 23761.6 2:1812.3 24027.9 BHV·2 Start 32324.2 32494.0 32663.0 32830.4 32995.9 33187.1 33334.8 33500.7 33667.5 33860.0 34001.3 34216.9 BHV·4 Stare 8320.0 8487.5 8654.6 8842.9 8990.8 9155.9 9323.7 9515.6 9657.3 9871.8 Total 10143.6 10060.8 9937.8 11485.2 8865.6 9897.6 10054.8 16997.4 3039.6 12934.8 7224.6 Total 10187.4 10143.0 10042.8 9928.2 11473.2 8863.8 9954.6 10006.8 11552.4 8477,4 12937.2 7222.2 Total 10053.0 10028.4 1\295.0 8872.8 990'.8 10071.0 11515.2 8500.2 12810.0 7299.6 Total Volume: 4.B3E+06 Total 10,627.686 10.540,935 10.4 12.065 12.033.312 9,288,696 10.341,920 10.506.177 17,760.441 3,150,231 13,332.328 7.446.635 loading, Per Cenl 0.0175 0.0170 0.0125 0.0075 0.0167 0.0134 0.0175 0.0128 0.016& 0.0173 0.01 14 Total Volume: 4.B2E+06 Total 10,529,339 10,627,058 10,522,076 10,402,007 12,020,739 9,2&6,810 10,401,478 10,46£.022 12,071,006 8,785,949 13,334,802 7,444.162 0.0238 0.0205 0.0174 0.0349 0.0309 0.0500 0.0438 0.0156 0.0365 Total Volume: 4.08E+06 Total 10,532,763 10,506.969 11.834.035 9,296,240 10,349,443 10,523,104 12,032,136 8,B09,578 13,265,537 7,523,940 Loading, Per Cent 0.0396 0.0223 0.D178 0.024B 0.0225 0.0271 0.0192 0.0149 0.0305 0.0045 Page f 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 37.0 37.0 37.0 37.0 37.0 36.9 36.9 '16.9 36.6 36.4 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 ]6.4 36.4 "1J OJ (Q CD '" '" o ~ '" w Week " 1 2 3 4 5 6 7 8 9 10 11 12 13 8HV-5 on stream % Filter Start ...... " ........ ~ ... , .... 8155035 05.Jul-1Q 8155028 12-Jul-l0 8155023 19-Jul-1O 8155019 26.Jul-l0 8155009 02-Aug-l0 8155003 09-Aug-l0 8153796 16·Aug-l0 8153790 23-Aug-l0 8153787 30-Aug-IO 8153781 06-Sep-IO 8153775 13-Sep-10 8153766 2Q-Sep-1O 8153760 27-Sep-l0 Totals 91 75.4% Stop ....... '" .... ' .... ,," 'a,,,, ,~'" 12·Jul-l0 4.6790 4.4594 0.2196 19-Jul-l0 4.7034 4.4781 0.2253 26-Jul-10 4.7470 4.5127 0.2343 02-Aug-l0 4.6643 4.4908 0.1735 OS-Aug-IO 4.6053 4.4989 0.1064 IS-Aug-l0 4.6559 4.4959 0.1600 23·Aug-l0 4.6362 4.4853 0.1509 30·Aug-IO 4.6685 4.4782 0.1903 06-Sep-l0 4.7436 4.4836 0.2600 13-Sep-l0 4.5538 4.5207 0.0331 2O-Sep--l0 4.51 16 4.4976 0.0140 27-Sep-l0 4.5082 4.5082 0.0000 04-0ct-l0 4.6416 4.4786 0.1630 2184.0 4.63988 4.49138 0.1485 BHY-S Total Volume: 3.64E+06 Stop Start Total Total Loading, Per Cent ''''''"' ""''"' ''''''"' .... , .. '''' 'I' ,,,'" ..... " .......... ". ........,. ,~. 32446.0 32279.5 9991.2 10,326,554 0.0213 99.1% 36.5 32616.9 32446.0 10251.0 10,740,212 0.0210 101.7% 37.0 32784.4 32616.9 10053.6 10,533,391 0.0222 99.7% 37.0 32951.3 32784.4 10012.2 10,490,016 0.0165 99.3% 37.0 33140.4 32951.3 11345.4 11.886,840 0.0090 112.6'% 37.0 33288.2 33140.4 8867.4 9,290,562 0.0172 88.0% 37.0 33453_3 33288.2 9906.0 10,350,697 0.Q146 98.3% 36.9 33620.5 33453.3 10036.2 10,486,742 0.0181 99.6% 36.9 33812.2 3362<l.5 11497.2 12,013,328 0.0216 114.1% 36.9 33842.9 33812.2 1841.4 1,908,421 0.0173 18.3% 36.6 33842.9 33842.9 0.0 a #DIV!OI 0.0"'10 36.' 33842.9 33842.9 0.0 0 #OIV!D! 0.0"10 36.4 33927.2 33842.9 5062.2 5,217.778 0.0312 50.2% 36.4 7797800 98863.8 103,244,560 #DIViO! 75.4% 36.8 '1J !ll <0 <D '" '" So '" '" Period: July 5,2010 through October 4, 2010 (3rd Quarter 2010) 8HV·6 on stream % Week Filter Start . '~U'''","",I Lleu.,- 1 8155034 05-Jul-l0 2 8155027 12-Jul-l0 3 8155022 19-Jul-l0 4 8155020 26-Jul-l0 5 8155008 02-Aug-l0 6 8155002 09-Aug-l0 7 8153795 16-Aug·10 8 8153789 23-Aug-l0 9 8153788 30-Aug·l0 10 8153782 06·Sep-10 11 8153776 13·Sep-l0 12 8153765 2O-Sep-l0 13 8153759 27-Sep·l0 Totals 91 ALL 8HV on stream % Week # Blanks Slart Date 1 8155032 05-Jul-l0 2 8155021 12-Jui-l0 3 8155014 19-Jui-l0 4 8155013 26-Jul-l0 5 6155007 02-Aug·l0 6 8153800 09-Aug-l0 7 8153794 16-Aug-l0 8 6153783 23-Aug-l0 9 8153777 3O-Aug-l0 10 8153771 06-Sep-l0 11 8153770 13-Sep-l0 12 8153764 20-Sep-l0 13 6153758 27-5eo-10 Totals 91 75.4% Stop .... ell\::" 12-JuJ-l0 19-Jul-l0 26-Jul-l0 02-Aug-l0 09-Aug-l0 16-Aug-l0 23-Aug-10 3O-Aug-10 06-Sep-l0 13-Sep-l0 2G-Sep-10 27-Sep-l0 04-0c1-10 2184.0 87.2% Stop Date 12-Jul-l0 19-Jul-l0 26-Jul-10 02-Aug-l0 09-Aug-l0 16·Aug-10 23-Aug-l0 30-Aug-l0 06-Sep-l0 13-Sep-10 2O-Sep-10 27·Sep-l0 O4-Oct-IO 2184.0 Stop '-"'v'"" ,a,lO '.':'1 '''', .. 4.6746 4.4789 0.1957 9498.6 4.7025 4.4543 0.2482 0069.5 4.7134 4.4978 0.2156 9837.1 4.6755 4.5018 0.1737 10003.8 4.6356 4.5167 0.,,89 10192.5 4.6561 4.4915 0.1646 10340.4 4.6396 4.4867 0.1529 10505.5 4.7013 4.4740 0.2273 10673.0 4.7864 4.5080 0.2784 10864.7 4.5056 4.4742 0.0314 10895.2 4.4895 4.4759 0.0136 10895.2 4.4948 4.4945 0.0003 108952 4.6263 4.4918 0.1345 10979.6 4.63855 4.48816 0.1504 Net 4.4840 4.4803 4.4772 4.5079 4.5113 4.4861 4.5071 4.4884 4.4837 4.4674 4.4826 4.4778 4.4864 4.4Bn Page 2 BHV-6 Total Volums: 3.63E+06 Start Tolal Total Loading. Per Cent '''" .. '''''''' ""'10::';' "' ''',;1 V"';>II',I<"III .,;!,-,rM 9332.0 9997.8 10.333,375 0.0189 99.2% 36.5 9498.6 10255.2 10,744,612 0.0231 101.7% 37.0 9669.5 10053.0 10,532,763 0.0205 99.7"10 37.0 9837.1 10002.6 10,479.957 0.Q166 99.2% 37.0 10003.8 11325.0 ",865.467 0.0100 112.4% 37.0 10192.5 8871.0 9,294,354 0.0177 88.0% 37.0 10340.4 9906.0 10,350,697 0.0148 98.3% 36.9 1050S.5 H)()49.4 10.500,534 0.0216 99.7% 36.9 10673.0 11506.2 12,022,732 0.0232 114.1% 36.9 10664.7 1825.2 1,891,831 0.0166 18.1% 3M 10895.2 0.0 0 #DIVlO! 0.0% 36.4 10695.2 0.0 0 #DIVlOI 0.0% 36.4 10895.2 5064 .• 5,219,633 0.0258 50.2% 36.4 98855.4 103,235,756 #DIV/O! 75_4% 36.8 W .. k 2 3 4 5 6 7 8 • 10 II 12 Week 2 3 4 5 6 7 8 9 10 11 12 13 Week 2 3 4 5 6 7 8 9 10 11 12 13 W .. k 2 3 4 5 6 7 8 9 10 11 12 13 Period: October 4, 2010 through January 3, 2011 (4th Quarter 2010) SHV·, on stream % Filler 8t53751 8153743 8153736 8153730 8153724 8153721 8400799 8400793 8400787 8153713 8400781 Start II·Oct·1O 18·Oct·IO 25·OcI·1O OI·Nov-IO OS-Nov·1D 15·Nov-to 22-Nov-1D 29-NQv-IO 06-0ec-1O 1)·Dec·1O 2Q...Dec-1O BHV·2 on stream % Filter 8153750 81 53742 8153737 8153731 8153725 8153720 8400796 6400792 8400786 8153712 8400780 6400n4 Start 1'-OcI-'0 lS·OcHO 25-Oct-l0 OI·Nov-l0 08-Nov-l0 15·Nov·l0 22-Nov-l0 29·Nov·l0 06-Dec-l0 13·0ec-IO 20-0ec-l0 BHV·4 on stream % Filler 8153749 8153744 8153738 8153732 8153726 8153719 6400797 8400791 8400785 6153714 8400ng 8400773 Slart 11-OcI-l0 18·Oct-10 25-OcI-l0 01-Nov-l0 08·Nov-tO 1 S-NoY-l 0 22·NoY·l0 29·Nov-10 06-Dec-tO 13·Dec-l0 20-0ec-l0 27-0ec·l0 BHV-5 on slream % Filler 8153748 8153745 8153739 8153733 8153727 8153716 8400796 8400790 8400764 8153715 8400778 51.rt 1'-Oct-l0 18·0ct-l0 25-Oct-l0 Ot·NoY-l0 08-NoY-l0 lS·Nov-IO 22-NoY-l 0 29-NoY-l0 OB·Dec-l0 13·Dec-l0 20-Dec·l0 102.2"4 Stop 18·Oct-JO 25-OcI-l0 I·Nov·JO 8-Nov-JO 15·Nov·1O 22-Nov-1O 29-Nov-JO 6·Dec-10 B -Oee·IO 2o-Dec·10 21-Dec-1O 100.9% Slop 18-0ct-l0 25-0cHO 01-Nov-l0 08·Noy-l0 15-NoY-IO 22-NoY-l0 29-NoY-l0 OS·Dec-l0 13-Dec-l0 20-Dec·l0 27-Dec-l0 03-Jan-l l 100.4% Stop 18-acHO 25·Qct-l0 01-NoY-l0 08-Nov-fO 15-NoY-10 22-NoY-l0 29·NoY-l0 06-0ec-l0 l3-Dec·l0 20-Dec-l0 27-Dec-l0 03-Jan·11 97.0"~ Stop 18·0ct-l0 25-Qct-10 Q1·Nov-l0 Oe-Nov-l0 IS-NoY-IO 22-NoY-l0 29-Noy-l0 OB-Dec-l0 13-Dec·l0 20·000-10 27-Dec·IO 84.0 4.6114 4.6300 4.6042 4.5985 4.5615 4.6649 4.3964 4.4149 4.3400 4.5650 4.3770 4.8884 4.6982 4.7117 4.8941 4.6425 4.6875 4.3874 4.5169 4.5942 4.9186 4.4028 4.4131 4.5621 4.5379 4.6317 4.5852 4.5446 4.6159 4.3800 4.3681 4.4135 4.6373 4.4345 4.3400 4.6539 4.5624 4.6310 4.6705 4.5668 4.6642 4.4145 4.4680 4.3913 4.6276 4.3672 4.4907 4.5162 4.4841 4.4963 4.4915 4.5022 4.3181 4.3232 4.2148 4.4828 4.301 1 4.5084 0.1201 0.1138 0.1195 0.1022 0.0100 0.1627 0.0783 0.0911 0.0652 0.0822 0.0753 4.4958 0.2024 4.5124 0.1993 4.4974 0.3967 4.4973 0.1452 4.4761 0.2114 4.2713 0.1161 4.3057 0.2112 4.3218 0.2724 4.4548 0.4638 4.3059 0.0969 4.3097 0.1034 4.5019 4.5102 4.5080 4.4708 4.4768 4.4715 4.3246 4.2792 4.3173 4.4844 4.3133 4.4987 4.4820 4.4977 4.5074 4.4867 4.5013 4.3409 4.3257 4.2629 4.4663 4.2623 0.0602 0.02n 0.1237 0.1144 0.0678 0.1444 0.0554 0.0889 0.0962 0.1529 0.1212 0.0244 0.1552 0.0804 0.1333 0.1631 0.0801 0.1629 0.0736 0.1423 0.1084 0.14 13 0.1049 Stop 24652.4 24824. I 24989.1 25158.0 25324.1 25491.5 25664.3 25833.3 25999.9 26168.1 26331.5 Stop 55013.7 35176.9 35347.1 35513.5 35666.1 35853.4 36022.5 36168.5 36358.0 36526.1 36712.9 Stop 10495.0 10666.0 10830.7 11000.8 11 167.4 11340.2 11507.3 11676.6 11835.5 12002.8 12170.9 12359.4 Stop 34180.7 34351.7 34516.6 34686.6 34853.1 35025.9 35192.4 35361.7 35521.2 35687.9 35656.1 Start 24483.5 24652.4 24824.l 24959.1 25 158.0 25324.7 25491.5 25664.3 25833.3 25999.9 26168.7 26337.5 BHV-2 Start 34509.1 34672.6 34840.9 35013.7 35176,9 35347.1 35513.5 35686.1 35853.4 36022.5 36188.5 36358.0 36526.1 BHV4 Start 10328.1 10495.0 10666.0 10830.7 11000.8 11167.4 11340.2 11507.3 11678.6 11835.5 12002.8 12170.9 SHY-S SJart 34018.6 34160.7 34351.7 34516.6 34686.6 34853.1 35025.9 35192.4 35361.7 35521.2 Total 10134.6 10302.0 9898.2 11935.8 10000.2 10366.8 10009.8 to14t.8 9996.0 10125.6 10130.4 11214.6 Total 9174.0 10095.6 10368.0 9793.8 10214.4 9979.8 10359.6 10036.2 10147.8 9959.4 10 168.8 10086.0 Total 10013.4 10259.4 9886.2 10206.6 9995.4 10368.0 10022.4 10162.2 9532.8 10034.4 10088.4 Total 9726.6 10261.8 9891.6 10204.8 9988.8 10365.6 9993.6 10153.8 9574.8 9997.8 10092.0 I Tolal Volume: Tolal 10,6 18,257 10.793.646 10,370,575 12,505,416 10.471,443 10.832,183 10,459.156 10.597,082 10,359.820 10,436.792 10,441,740 4.92E ... OO Loading, Per Cent 0.0114 0.0105 0.0115 0.0082 0.0067 0.0150 0.0075 0.0087 0.0063 0.0079 0.0072 100 . .5% 102.2% 98.2% 118.4% 99.2% 102.8% 99.3% 100.6% 99.2% 100.5% 100.5% Tolal Volume: 4.66E+06 Total 10,102,063 10,577,396 10,862,796 10.261,193 10.701 ,865 10,456,069 10,824,660 10,486,742 10,603,352 10,321 ,888 10,481.320 10,395,975 Loading, Per Cent 0.0166 0.0194 0.0371 0.0139 0.0195 0.0111 0.0199 0.0264 0.0443 0.0093 100.2"k 102.9% 97.2% 101.3% 99.0% 102.8% 99.6% 100.7% 98.8% 100.9% 100.1% Total Volume; 4.84E+OS Total 10,491 ,273 10.749,013 10,358,002 10,693,693 10,472,414 10,833,437 10.472,322 10,618,398 9,879,762 10.342,790 10,396,449 Loading, Per Cent 0.0057 0.0026 0.0119 0.0107 0.0065 0,0133 0.0053 0.0084 0.0097 0.0148 0.0117 99.3% 101.8% 98.1% 101.3% 99.2'Y .. 102.90/0 99.4% 100.8% 94.6% 99.5% 100,1% Total Volume: 4.67E ... 06 Tolal 10,190,786 10,751,527 10,363,660 10,691,807 10.465,499 10,830,929 10,442.229 10,609,621 9,923,290 10,305.065 10,402,160 Loading, Per Cent 0.0152 0.0075 0.0129 0.0153 0.0077 0.0150 0.0070 0.0134 0.0109 0.0137 0.0101 96.5% 101.8% 98.1% 101.2% 99.1% 102.8% 99.1% 100.7% 95.0% 99.2% 100.1% 97.0% Page 1 17.0 37.0 37.0 37.0 37.0 36 .• 36.9 36.9 36.6 36.4 36.4 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36 .• 36.6 36.4 36.4 37.0 37.0 31.0 31.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 37.0 37.0 31.0 37.0 37.0 36 .• 36.9 36.9 36.6 36.4 36.4 Period: October 4, 2010 through January 3,2011 (4th Quarter 2010) Pag92 8HV·6 on stream % 83.6% BHV"; Tolal Volume: 4.03E+06 Week Filler Star1 Stop Stop Star1 Total Total Loading, Per Cent 2 81 53747 11·Oct·l0 18-Oct-l0 4.7006 4.5036 0.1970 176.2 12.6 9814.2 10,282,566 0.0192 97.4% 37.0 3 8153746 18-Oct-10 25-0ct-l0 4.5707 4.5052 0.0655 347.2 176.2 10260.6 10,750,270 0.0061 101.8% 37.0 4 8153740 25·Qc1·10 01·Nov-IO 4.6320 4.5128 0.1192 512.0 347.2 9888.6 10,360,517 0.011 5 98.1% 37.0 5 8153734 Ot-Nov·tO OS·Nov·l0 6.6356 4.5119 2.1237 682.1 512.0 10202.4 10,689,293 0.1987 101.2% 37.0 6 6153728 08·Nov·tO 1 S-Nov-l 0 4.5625 4.4845 0.0780 848.6 682.1 9994.2 10,471,157 0.0074 99.1% 31.0 7 8153717 I S-Nov-I 0 22-Noy·IO 4.6500 4.4614 0.1666 1021.1 848.6 10348.2 10,812,748 0.0156 102.7% 36.9 8 8400795 22-Nov-l0 29-Nov-lo 4.3748 4.3010 0.0738 1188.2 1021.1 10021.2 10,477,338 0.0070 99.5% 36.9 9 8400789 29-Nov-10 06-0ec-l0 4.4593 4.3265 0.1328 1357.5 1188.2 10151.4 10,613,382 0.0125 100.8% 36.9 10 8400783 OS-Oec-IO 13·0 ec·l0 4.3943 4.3139 0.0804 1471.9 1357.5 6864.6 7.114.448 0.0113 68.1% 36.6 11 8153716 13-Dec-l0 20-0ec-IO 4.5203 4.4768 0.0435 1536.5 1471.9 3814.2 3,993.267 0.0109 38.4% 36.4 12 8400777 20-0ee-I O 27-0ec-l 0 4.3881 4.3223 0.0658 1636.2 1536.5 5982.0 6.165,646 0.0107 59.3% 36.4 ALL BHV on stream % 96.8% Week Start Stop 2 8153741 11-Oct·l0 16·0ct-l0 4.5067 3 6153735 ta-OcI·l0 25·Oct-l 0 4.4000 4 6153729 25-0cHo 01-Noy-10 4.4800 5 8153723 01-Nov-tO 08-Nov-10 4.4755 6 8153722 OS-Nov-l0 l 5-Nov-10 4.4934 7 8400800 15-Nov-l0 22-Nov-10 4.3225 8 8400794 22-Nov-l0 29-Nov-10 4.3040 9 8400766 29-Nov-l 0 OB·Dec-l0 4.3008 10 8153711 06-Dec-10 13-0ec-10 4.4844 11 6400782 13·Dee-tO 20-Dec-tO 4.3276 12 8400776 20·Dec-l0 27·0ec-10 4.2791 ATIACHMENT E ENVIRONMENTAL GAMMA (TLD) GRAPHS AND SUPPORTING DATA 50.00 45.00 40.00 35.00 30.00 ~ Q) 1:: ctJ 25.00 :J ~ E Q) a:::: 20.00 E 15.00 I White Mesa Mill Ambient Gamma Levels Over Time I 10.00 j---tl • "-I·I--------------::c--- 5.00 0.00 30-Se1J..81 3o..Sep..9Q 30_Sep..99 3o..SeP-08 Background (BHV-3) subtracted from BHV-1. BHV-2, SHV4, SHY-5, and BHV-6 ~BHV·1 ~BHV·2 -a--BHV·3 _BHV4 _BHV-5 ~BHV-6 I White Mesa Mill Ambient Gamma Levels Over Time BHV-11 50.00 45.00 40.00 35.00 30.00 ~ Q) 1:: <1l 25.00 ::J !?: E Q) c::: 20.00 E 15.00 10.00 -J ~ "",; " j} ,-~~ .[--'AN\fi1 A .• .. AAA .. ~ - 5.00 0.00 3D-SeP-81 30-Sep_90 30·Sep..99 3o.SeP-08 Background (BHV-3) Subtracted from BHV-1 r-------------------------- -+-BHV-1 I White Mesa Mill Ambient Gamma Levels Over Time BHV-2J 50.00 45.00 40.00 35.00 +1-------------------------------------------1 30.00 '-Q) t:: 25.00 co :::J -S! E Q) a::: 20.00 E 15.00 10.00 I • 5.00 I 11' II II W • _ _'Il10 JI'" 0.00 30-Sep_81 30-Sep_90 30-Sep_99 30-Sep_08 Background (BHV-3) Subtracted from BHV-2 __ BHV-2 I White Mesa Mill Ambient Gamma Levels Over Time ·-SHV-3] 50.00 45.00 40.00 35.00 30.00 ~ Q) 1:: 25.00 CtI ::::J c;r -E Q) 20.00 0:: E ~ rJ I ~ lf1._rt ~ --, ~ I.~r ~~~~~ ~ I ~ r 1\~ It, • ~--~-, ~,--~ 15.00 10.00 5.00 0.00 30·Sep..a, 30•SeP.90 30·SeP.99 30-SeP-08 Background (BHV·3) r------------------ - ----.-BHV-3 I White Mesa Mill Ambient Gamma Levelsch;riime BHV-4] 50.00 45.00 40.00 35.00 30.00 ~ OJ 25.00 1:: C\l :::l rr -E OJ 20.00 c::: E 15.00 10.00 5.00 0.00 30·SeP.81 30-SeP-90 30·SeP.99 30·Se1J.08 Background (BHV-3) Subtracted from BHV-4 -+-BHV-4 --~ I White Mesa Mill Ambient Gamma Levels Over Time BHV-sl ~.OO .-----------------------------------------------------------------------------------------------, 45.00 11------------------------------------------------------------------------------------------- 40.00 +1------------------------------------------------------------------------------------------ 35.00 1----------------------------------------------------------------------------------------- ~.OO 1--------------------------------------------------------------------------------- ~ 20.00 1 E 15.00 1------------------------------------------------------------------------------------------1 1~i t :~~ 3o..SeP.81 3()..Sep.90 Jo..Sep.9g JD..seP-()8 Background (BHV-3) Subtracted from BHV-5 [ -+-SHV-5 -------- ! White Mesa Mill Ambient Gamma Levels Over Time BHV-S! 50.00 45.00 40.00 35.00 30.00 ~ Q) 25.00 1:: til :::l -!! E 20.00 Q) n:: E 15.00 10.00 5.00 0.00 ~ A.J 30•SeP-81 30-Sep.SO 30-S0P.99 30-S°P-08 Background (BHV-3) Subtracted from BHV-6 [ -------+-SHV:'; Badge Number o 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 Location of Spherical Environmental Monitors Location of Monitors Administration Building -Vault (Control) Vanadium Control Room -Located on South Wall BHV-6 Ore Storage -Cameco Barrel Storage Area Vanadium Precipitation -Located on Agitator Start Stop Button Yellowcake Drying Area -Located on North Yellowcake Dryer Alarm Leach Area -Located at #2 Leach Tank Eyewash Station Derrick Screens -northeast comer Yellowcake Precip. -Located on S. Wall by Yellowcake Acid Redissolve Tank Central Control Room -Located on Shifter's Bulletin Board Ore Pad -Decontamination Pad Barrel Dump Station -Located at Operator's Panel Metallurgical Laboratory -Hanging From Ceiling Filter Press Room -Located on North Wall BHV-I BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill -Located Outside SAG Mill Control Room Door (North Side) Tails -Located on Cell 2 at the Power Distribution Center CCD -Located Outside MCC On North Wall on Breaker Box North SX -Located on Regen. Pump Start/Stop Switch Administration Building -Located on Main Bulletin Board In Tree By Picnic Bench Outside Administration Building Yellowcake Packaging -Hung on Wall outside Door North Yellowcake Dryer Area 2nd Level on N. Dryer Temp. Ctr!' Box Bucking Room -Located on East Wall Behind Crusher Mill Lunch Room -Located on Projection Screen on West Wall South SX -Located on Column # I 0 Electrical Foreman's Office -Located on North Wall Ore Feed Grizzly -Located on North Wall at Power Distribution Boxes Scalehouse -Located in Office at Northeast Comer OBS (Sample Plant) -Located on South Side of Southwest Entrance Door Front Gate Alternate Feed circuit -Barrel Dump Station Alternate Feed Circuit -Start/Stop Switch Sump Pump Southwest Alternate Feed Circuit -Start/Stop Switch Sump Pump Impurity Removal Tanks Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 White Mesa Mill Third Quarter 2010 Environmental Spherical Gamma Monitor Results Mean Location Administration Vault V205 Control Room BHV-6 Ore Stor. -Molycorp Area Vanadium Precip.Area Yellocake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room Trommel Screen (ore pad) Barrel Dumping Station Met. Lab Filter Press Room BHV-I BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scalehouse Sample Plant (OBS) Front Gate AF -Barrel Dump Station AF -South Side AF -North Side Date Issued 7/6/2010 7/6/2010 7/612010 7/6/2010 7/612010 7/6/2010 7/6/2010 7/6/2010 7/6/2010 7/6/2010 7/6/2010 7/612010 7/612010 7/612010 7/6/2010 7/612010 7/612010 7/612010 7/612010 7/6/2010 7/6/2010 7/6/2010 7/6/2010 7/612010 7/612010 7/6/2010 7/6/2010 7/612010 7/612010 7/612010 7/612010 7/612010 7/612010 7/6/2010 7/6/2010 7/6/2010 7/612010 7/6/2010 Date Returned 9/30/2010 9/30/2010 9/3012010 9/30/2010 9/3012010 9/3012010 9/3012010 9/3012010 9/30/2010 9/3012010 9/3012010 9/3012010 9/3012010 9/3012010 9/3012010 9/3012010 9/30/2010 9/3012010 9/3012010 9/30/20 I 0 9/3012010 9/3012010 9/30/2010 9/30/2010 9/3012010 9/3012010 9/3012010 9/3012010 9/3012010 9/3012010 9/3012010 9/3012010 9/30/2010 9/30/2010 9/30/2010 9/3012010 9/30/2010 9/30/2010 Total Days Badge at WMM 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 86 Ambient Dose Equivalent 29.8 43.6 20.5 805.8 84 195 189.8 211.3 138.7 79.4 239 484.8 57.3 146 29 24.8 21.6 20.4 28.1 253.7 113.7 67.4 77.6 29.8 89.5 940.4 400.9 98.1 57 156.2 42.3 323.2 223.5 199.8 217.5 122.9 68.8 274.8 mReml hour 0.01 0.02 0.01 0.39 0.04 0.09 0.09 0.10 0.07 0.04 0.12 0.23 0.03 0.07 0.01 0.01 0.01 0.01 0.01 0.12 0.06 0.03 0.04 om 0.04 0.46 0.19 0.05 0.03 0.08 0.02 0.16 0.11 0.10 0.11 0.06 0.03 0.13 mReml Day 0.347 0.507 0.238 9.370 0.977 2.267 2.207 2.457 1.613 0.923 2.779 5.637 0.666 1.698 0.337 0.288 0.251 0.237 0.327 2.950 1.322 0.784 0.902 0.347 1.041 10.935 4.662 1.141 0.663 1.816 0.492 3.758 2.599 2.323 2.529 1.429 0.800 3.195 mReml Week 2.43 3.55 1.67 65.59 6.84 15.87 15.45 17.20 11.29 6.46 19.45 39.46 4.66 11.88 2.36 2.02 1.76 1.66 2.29 20.65 9.25 5.49 6.32 2.43 7.28 76.54 32.63 7.98 4.64 12.71 3.44 26.31 18.19 16.26 17.70 10.00 5.60 22.37 Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 White Mesa Mill Fourth Quarter 2010 Environmental Spherical Gamma Monitor Results Mean Location Administration Vault V205 Control Room BHV-6 are Stor. -Molycorp Area Vanadium Precip.Area Yellocake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room Trommel Screen (ore pad) Barrel Dumping Station Met. Lab Fi lter Press Room BHV-I BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room M ill Lunch Room South SX Mtce. Super.'s Office a re Feed Grizzly Scalehouse Sample Plant (OBS) Front Gate AF -Barrel Dump Station AF -South Side' AF -North Side' Date Iss ued 9/30120 10 9/3012010 9/30120 10 9/30120 10 9/30/2010 9/30/20 10 9/3012010 9/30/20 10 9/30120 10 9/3012010 9/30120 10 9/30120 10 9/30120 10 9/30120 10 9/30/20 10 9/30/20 10 9/30/2010 9/30/2010 9/30/20 10 9/30120 10 9/30/20 10 9/30/20 10 9/30/2010 9/30/20 10 9/30/20 10 9/30/20 10 9/30/2010 9/30/20 10 9/30/20 10 9/30120 10 9/30120 10 9/30/20 10 9/30/20 10 9/30/20 10 9/30120 10 9/30120 10 9/30/2010 9/30/2010 Total Days Badge at Date Returned WMM 117120 II 99 117120 II 99 11712011 99 117120 11 99 117120 II 99 117120 II 99 117120 II 99 117120 II 99 1171201 1 99 117120 II 99 117120 II 99 11712011 99 11712011 99 117120 II 99 11712011 99 11712011 99 11712011 99 117120 11 99 117120 11 99 117120 11 99 117120 II 99 1171201 1 99 117120 11 99 117120 11 99 11712011 99 117120 11 99 1171201 1 99 11712011 99 117120 11 99 117120 11 99 117120 11 99 117120 11 99 117120 11 99 117120 11 99 117120 11 99 117120 11 99 117120 11 99 117120 11 99 Ambient Dose mRem l Equivalent hour 37 0.02 58.4 0.02 31.7 0.01 924.9 0.39 109.2 0.05 145.3 0.06 308.3 0.13 398.2 0.17 97.1 0.04 89.8 0.04 277.3 0.12 167.1 0.07 79.1 0.03 2 19.7 0.09 35.5 0.01 36.7 0.02 31.1 0.01 34.7 0.01 37 0.02 528.9 0.22 124 0.05 87.7 0.04 91.2 0.04 41.9 0.02 91.8 0.04 893.4 0.38 423.6 0.18 122.1 0.05 59.7 0.03 170.7 0.07 52.5 0.02 41 2.9 0.17 201.1 0.08 257.7 0.11 2 10.1 0.09 143.1 0.06 0.00 0.00 mRem l Day 0.374 0.590 0.320 9.342 1.1 03 1.468 3.114 4.022 0.98 1 0.907 2.80 1 1.688 0.799 2.2 19 0.359 0.37 1 0.3 14 0.351 0.374 5.342 1.253 0.886 0.92 1 0.423 0.927 9.024 4.279 1.233 0.603 1.724 0.530 4.171 2.031 2.603 2.122 1.445 0.000 0.000 * Lost Badge mRem l Week 2.62 4.13 2.24 65.40 7.72 10.27 21.80 28.16 6.87 6.35 19.61 11.82 5.59 15.53 2.5 1 2.59 2.20 2.45 2.62 37.40 8.77 6.20 6.45 2.96 6.49 63.17 29.95 8.63 4.22 12.07 3.71 29.19 14.22 18.22 14.86 10.12 0.00 0.00 ATTACHMENT F VEGETATION GRAPHS, DATA TABLE, LABORATORY RESULTS AND QAJQC (Log Scale) ~ ~ ~ ~ o a a a a a a 000 a a 0 a m m m m m m m I , , , I I I 000 a a 0 0 ~ ~ m ~ ~ W N 8/27/1981 8/27/1982 I..L'" ,,~=-+ 8/27/1983 ~rP' 8/27/1984 ~ 8/27/1985 K: ~ 8/27/1986 ~ 8/27/1987 ~ 8/27/1988 _ "' ~ • 8/27/1989 ~ ~ 8/27/1990 /-b g 8/27/1991 -tI' g ::l 8/27/1992 --~ ~ 8/27/1993 --~ o· 1 _~~~::l T 8/27/1994 . U> Z ~ ::l m 8/27/1995 ~~ ~ T 8/27/1996 ~ .'"' ~ z 8/27/1997 r .4 ~ ~ g 8/27/1998 . -=:::: ~ ,t( ". -:::::. ~ t 8/27/1999 -..< .. -~ ~ ~ m~oo k 8 mn~1 ~ ~ 8/27/2002 . .. 8/27/2003 :::- 8/27/2004 ~ 8/27/2005 ~ 8/27/2006 ~ 8/27/2007 .......;:-- 8/27/2008 ..::;;-~--- 8/27/2009 .... L --:..:... 8/27/2010 L / ,../ (Log Scale) ~ ~ ~ a a a a a a a 0 0 0 0 0 0 0 m m m m m m m , , 6 , , , 6 0 0 0 0 0 co -.J '" '" .,. '" '" 8/27/1981 ............. J.i 8/27/1982 .. ~ ~ 8/27/1983 .c: !S: 8/27/1984 ~ .... --¥ 8/27/1985 8/27/1986 K ~X- -L 8/27/1987 ~ ~ "'C 8/27/1988 ---c-o 8/27/1989 ~ N .... I~ ~ 0 8/27/1990 -0 0 :::l 8/27/1991 -n (1) :::l 8/27/1992 /" -iil -8/27/1993 Jl"\ ci" t :::l 8/27/1994 en z t;p' :::l m 8/27/1995 r=::::~ < (1) T cc 8/27/1996 ... ~ (1) -III -z 8/27/1997 ci" ::! :::l 8/27/1998 ~ ~ c t 0 8/27/1999 ::::: ;lI; (f) ~, cc ::! 8/27/2000 - ---- ~ 8/27/2001 - "\."'" ~ 8/27/2002 8/27/2003 --...",. 8/27/2004 8/27/2005 8/27/2006 I~ 8/27/2007 -» 8/27/2008 ::,.. ~ 8/27/2009 ~"'" r- 8/27/2010 ~ (Log Seal.\!) ~ ~ ~ a a a a a a a 0 0 0 0 0 0 0 m m m m m m m 6 , 6 , 6 , 6 0 0 0 "" .... 0) '" ... w '" 01-Jan-8 1 01-Jan-82 ~ Ir A :E :I: 01 -Jan-83 l ::::j m 01-Jan-84 3: m 01-Jan-85 i ~ ____ I (Jl » ,,",,-M 1 .~ 3: I"" 01-Jan-87 I"" 01 -Jan-88 Z 0 01-Jan-89 i r----....-----...J. ;;0 --I :I: 01-Jan-90 i ~ m » 01-Jan-91 i l.r ~ (Jl --I 01-Jan-92 0 t 'TI 01 -Jan-93 3: ;u I"" '" ~I"" , 01-Jan-94 f,;;o '" '" Ol •. I» 01-Jan-95 -0 T ;:11:;1\) CCI\) 01-Jan-96 ~ en -u I» ~ :l 01-Jan-97 0.. ~ 0 "C 01-Jan-98 c-o I\) ..... 01-Jan-99 -I 1 ~ 1 0 C'l 01-Jan-OO -0 :l -t V .--0 01-Jan-01 (1) :l .... o 1-Jan-02 -I ~=----.... I» .... o 1-Jan-03 -I ~J o· :l III 01 -Jan-04 --=' ~ :l 01-Jan-05 -I -~ < (1) cc 01-Jan-06 -I .. -"'1 (1) -.... I» .... 01 -Jan-07 1 I +<:::::::_ f<" I o· :l 01-Jan-08 01-Jan-09 01-Jan-10 ~ ~ 0 0 0 0 0 0 m m m , , , 0 0 0 00 ...., Ol 01-Jan-81 01-Jan-82 01-Jan-83 01-Jan-84 01-Jan-85 01-Jan-86 01-Jan-87 01-Jan-88 01-Jan-89 01-Jan-90 01-Jan-91 tl 01-Jan-92 i?i'l 01-Jan-93 ~ ~I 01-Jan-94 01-Jan-95 ;\1 1 01-Jan-96 ~ ~ 01-Jan-97 01-Jan-98 01-Jan-99 01-Jan-OO 01-Jan-01 01-Jan-02 01-Jan-03 01-Jan-04 01-Jan-05 01-Jan-06 01-Jan-07 01-Jan-08 01-Jan-09 01-Jan-1 0 (Log Scale) ~ ~ 0 0 0 0 0 0 m m m , 6 , 0 0 01 ... '" ~ 0 0 m , 0 '" :E ::I: :::::j m s: m ~ s: r r z o ~ ::I: :E m (f) -I o ." s: r "2 r (");0 _.1\) -, ;l'i;N CON ~cn I\) :::l C. "'\J c-, N .... o (") o :::l o II) :::l r+ ~ o· :::l til :::l ~ CO ~ r+ o· :::l (Log Scale) ~ ~ ~ ~ ~ ~ 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m m m , b , , , b b , + 0 0 0 0 0 0 00 ..., (j> '" ~ W N ~ 0 01-Jan-81 1 I I k ls I; I I 1 :E :I: ::::j 01-Jan-82 m 01-Jan-83 3: 01-Jan-84 m CJ) 01-Jan-85 > 3: 01-Jan-86 r r 01-Jan-87 CJ) 01-Jan-88 0 c: ..... 01-Jan-89 ~ Is I;: I :I: :E 01-Jan-90 m CJ) 01-Jan-91 ..... 0 t 01 -Jan-92 " 3: JJ 01-Jan-93 r Ol , '2 r N N 01 -Jan-94 0;0 (j> _. III -0 T 01 -Jan-95 "N CON ~ Cl -u 01-Jan-96 III 'i" ::l N 01-Jan-97 Co ~ 0 "tI 01-Jan-98 c-o N .... "","-99 1 1 Ikf 0 0 01-Jan-OO 0 ::l 01-Jan-01 0 (1) ::l I ~ I .... 01-Jan-02 ~ ..... III .... 01-Jan-03 o· ::l ,,",,« 1 l ·1& UI ::l 01-Jan-05 ~ co 01-Jan-06 (1) .... III 01-Jan-07 i ~I 'I .... o· 01-Jan-08 ::l 01-Jan-09 01-Jan-10 WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHEAST OF MILL SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd '82 15-Apr-82 3rd '82 01-Jul-82 4th '82 3D-Nav-82 2nd '83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-84 2nd '85 27-Mar-85 3rd '85 15-Jul-85 4th '85 09-0ct-85 2nd '86 24-Mar-86 3rd '86 10-Jul-86 4th '86 lS-Dee-86 2nd '87 20-Apr-87 3rd '87 OS-Jun-S7 4th '87 22-Dec-87 2nd '88 19-Apr-88 3rd '88 28-Jul-88 2nd '89 07-Apr-89 3rd '89 06-Jun-89 4th '89 Ol-Nav-89 1st '90 17-Apr-90 2nd 'gO 20-Jun-90 3rd '90 17-0ct-90 1st '91 lO-Apr-91 2nd '91 ll-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 lO-Jun-92 3rd '92 lO-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd '93 12-0ct-93 1st '94 ll-May-94 2nd '94 19-Jul-94 3rd '94 28-Nov-94 1st '95 1l-Apr-95 2nd '95 06-Jul-95 3rd '95 lS-Nov-95 1st '96 23-Apr-96 2nd '96· 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd '97 05-5ep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 OS-Nov-98 2nd '99 15-Apr-99 3rd '99 07-Jul-99 4th '99 02-0ec-99 2nd '00 21-Apr-00 2nd '00 22-Jun-OO 4th '00 21-0ec-OO 1st '01 30-Apr-Ol 2nd '01 14-Jun-Ol 4th '01 17-0ec-Ol Ra-226 VALUE (uCi/Kg) 3.90E-04 1.40E-04 1.31E-04 1.60E-04 2.67E-06 9.36E-05 1.12E-04 1.09E-04 3.47E-04 5.61E-04 1.0sE-03 8.20E-05 1.15E-04 5.72E-04 5.01E-04 8.70E-04 5.90E-04 1.60E-04 2.10E-04 4.50E-04 3.20E-05 s.60E-04 1.50E-04 6.00E-04 2.60E-04 1.80E-04 1.60E-04 1.20E-04 9.10E-05 4.50E-04 3.60E-05 1.00E-05 7.90E-05 3.70E-05 3.00E-05 6.60E-05 1.80E-04 1.71E-05 2.40E-04 6.70E-05 1.50E-05 5.50E-05 5.20E-05 3.00E-05 1.10E-05 1.lOE-05 8.00E-06 <9.10E-05 1.80E-05 5.70E-05 2.00E-04 6.03E-05 2.30E-05 1.50E-04 1.20E-06 1.60E-06 1.00E-06 2.30E-06 9.10E-06 Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCI/Kg (5.0E-OS) VALUE (uCI/Kg) ERROR (uCI/Kg) uCI/Kg (1.0E-06) 1.0E-05 5.0E-08 1.10E-03 1.0E-04 1.0E-06 1.0E-05 5.0E-08 6.80E-04 8.0E-05 1.0E-06 1.3E-05 1.0E-06 4.90E-04 7.0E-05 8.0E-Os 1.0E-05 5.0E-08 8.00E-04 1.7E-04 1.0E-07 1.lE-06 1.0E-06 1.08E-04 9.0E-06 1.OE-05 6.2E-06 8.0E-09 4.97E-04 9.3E-05 1.0E-04 1.2E-Os 6.0E-06 1.84E-04 1.2E-05 1.0E-06 8.0E-06 4.0E-06 7.80E-04 6.2E-05 6.0E-05 1.2E-05 2.0E-09 3.75E-03 1.6E-04 4.0E-08 2.0E-04 2.0E-07 7.82E-03 3.3E-04 7.0E-08 3.0E-Os 2.0E-06 3.22E-03 1.4E-04 2.0E-05 7.0E-06 3.0E-06 7.70E-04 1.3E-04 2.0E-04 1.0E-05 3.0E-06 5.lOE-04 3.0E-05 2.0E-05 2.1E-Os 4.0E-06 2.49E-03 1.0E-04 1.0E-05 1.3E-05 3.0E-06 1.57E-03 1.7E-03 2.0E-04 5.0E-05 3.0E-06 6.80E-04 3.0E-05 3.0E-06 7.0E-05 5.0E-08 1.50E-03 1.0E-04 1.0E-06 3.0E-05 5.0E-08 9.50E-04 4.0E-05 1.0E-06 4.0E-05 5.0E-08 1.70E-03 1.0E-04 1.0E-06 7.0E-05 5.0E-08 1.40E-03 1.0E-04 1.0E-06 2.2E-Os 5.0E-08 1.50E-04 4.4E-04 1.0E-06 4.0E-Os ... 1.10E-03 1.0E-Ol ... 2.OE-05 ... 2.30E-04 2.0E-05 ... 5.0E-05 7.0E-06 2.04E-03 7.0E-05 1.4E-05 3.0E-Os 4.0E-06 3.30E-04 2.0E-05 2.2E-05 2.0E-05 5.0E-08 3.20E-04 2.0E-05 1.0E-06 2.0E-05 5.0E-08 3.30E-04 2.0E-05 1.0E-06 2.0E-Os 5.0E-06 3.ooE-04 2.0E-05 1.0E-06 1.6E-05 2.0E-07 1.90E-04 2.0E-Os 2.0E-07 4.0E-05 5.0E-08 1.09E-03 s.OE-05 1.0E-06 1.0E-05 2.0E-06 1.50E-04 2.OE-05 1.0E-05 7.0E-06 2.0E-07 7.50E-05 2.0E-Os 1.0E-06 3.5E-05 3.0E-06 7.10E-04 7.0E-05 2.0E-05 2.2E-05 3.0E-06 2.80E-04 3.0E-05 2.0E-05 1.5E-05 3.0E-06 4.30E-05 3.sE-Os 2.0E-05 2.7E-05 3.0E-06 5.30E-04 6.0E-05 2.0E-05 4.0E-05 3.0E-05 4.40E-04 6.0E-05 2.0E-04 1.2E-06 9.0E-08 3.00E-05 6.1E-06 4.5E-06 1.5E-Os 1.7E-07 1.70E-04 l.lE-05 8.3E-07 5.4E-06 1.6E-07 1.40E-04 1.3E-05 7.9E-07 1.5E-06 1.5E-07 5.10E-05 4.5E-06 7.6E-07 5.0E-06 1.8E-07 6.70E-05 1.0E-05 8.8E-07 2.5E-06 1.sE-07 3.20E-05 4.5E-06 1.8E-07 2.5E-06 1.8E-07 1.40E-04 7.1E-06 9.3E-07 4.7E-07 1.2E-07 4.lOE-05 3.6E-06 6.1E-07 4.3E-07 1.3E-07 2.10E-05 7.3E-07 6.7E-07 1.2E-06 5.6E-07 1.40E-04 4.6E-06 l.lE-07 9.1E-05 9.1E-05 <4.50E-04 4.5E-04 4.5E-04 1.2E-06 6.3E-08 4.00E-05 1.8E-06 3.2E-07 1.0E-06 S.2E-OS S.70E-05 5.0E-06 4.1E-07 3.0E-06 1.2E-07 3.00E-04 1.OE-05 6.0E-05 1.4E-06 8.3E-OS 1.40E-04 4.7E-06 4.2E-07 1.0E-06 2.3E-07 2.10E-05 1.0E-06 l.lE-06 3.0E-06 1.2E-07 1.60E-04 S.OE-06 5.9E-07 1.0E-07 2.8E-07 1.60E-04 1.0E-05 1.4E-06 1.1E-06 3.7E-07 5.lOE-05 5.0E-06 1.9E-06 1.0E-07 2.4E-07 <1.2E-06 1.0E-07 2.4E-07 2.0E-07 9.9E-08 3.S0E-06 2.0E-07 5.0E-07 2.4E-06 1.2E-07 3.57E-05 3.0E-06 6.0E-07 1st '02 07-May-02 3.30E-OS l.8E-06 7.6E-07 4.50E-OS 2.6E-06 !.OE-OS 2nd '02 07-Jul-02 S.5SE-OS 2.8E-06 7.6E-07 S.3IE-OS 3.9E-06 !'OE-OS 4th '02 1S-0ec-02 7.7SE-OS 3.6E-06 7.6E-07 !.29E-04 6.2E-06 !.OE-OS 1st '03 21-Mar-03 9.IOE-06 !.3E-06 3.6E-07 !.13E-OS !.6E-06 3.4E-06 2nd '03 10-Jun-03 2.50E-OS !.3E-06 3.6E-07 3.26E-06 2.0E-06 7.4E-OB 4th '03 20-Nov-03 S.70E-OS 3.5E-06 !.SE-07 4.0SE-OS S.BE-06 B.3E-07 1st '04 OB-Apr-04 9.3BE-OS 3.7E-06 l.lE-07 S.BBE-OS 3.0E-06 S.SE-07 2nd '04 12-Jun-Q4 S.63E-OS 3.4E-06 !.BE-07 6.42E-OS S.9E-06 9.0E-07 4th '04 30-Nov-04 B.4IE-OS S.50E-06 2.00E-OB 2.4BE-04 1.40E-OS 3.00E-07 1st '05 21-Apr-OS S.60E-OS 3.00E-06 !.40E-07 S.BOE-OS 4.00E-06 6.90E-07 2nd 'OS 13-Jun-05 9.IOE-06 1.50E-06 !.BOE-07 !'IOE-OS !.20E-OS 9.00E-07 4th 'OS 10-Nov-OS 6.00E-OS 3.00E-06 1.10E-IO 1.70E-06 6.40E-07 S.SOE-IO 1st '06 03-Apr-06 B.OOE-OS S.00E-06 S.OOE-OB 3.40E-04 1.20E-OS !.00E-06 2nd '06 16-Jun-06 4.IOE-OS 3.IOE-06 S.OOE-OB 1.16E-04 6.IOE-06 !'00E-06 4th '06 28-Nov-06 1.17E-04 4.60E-06 !.90E-07 3.2BE-04 9.50E-06 9.S0E-07 1st '07 30-Mar-07 9.70E-OS 4.40E-06 !.90E-07 3.40E-04 B.70E-06 B.4-07 2nd '07 1-Jun-07 !.30E-OS 1.60E-06 !.90E-07 !.20E-04 6.60E-06 9.70E-07 4th '07 23-Nov-07 7.00E-OS B.20E-06 2.00E-07 S.OOE-04 2.00E-OS !.20E-06 1st '08 22-Apr-OB 3.6E-06 3.00E-06 S.20E-07 2.3E-04 !.40E-OS !.OOE-06 2nd'OB 18-Jun-08 3.2E-OS 3.20E-06 !.80E-06 6.9E-OS 3.50E-OS S.50E-OS 4th 'OB 12-Doc-OB 1st '09 2B-Apr-09 S.9E-04 !.3SE-OS !.SOE-06 3.4E-04 !.30E-OS 1.50E-06 2nd '09 17-Jun-09 1.9E-OS I.4SE-06 4.90E-07 3.6E-OS !.IOE-OS !.BOE-OS 4th '09 IB-Doc-09 !.7E-04 S.90E-06 4.BE-04 !.20E-OS 1st '10 13-May-1O 2.2E-04 7.20E-06 1.10E-06 !.9E-04 !.90E-OS 2.90E-OS 2nd '10 18-Jun-IO 6.SE-OS 3.40E-06 7.60E-07 !.4E-04 !.90E-OS 2.90E-OS 4th '10 20-0ec-IO 2.3E-OS !.70E-06 S.20E-07 !.OE-OS !.SOE-06 2.30E-06 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period WHITE MESA MILL FORAGE RADIO NUClIDE DATA NORTHWEST OF MILL SAMPLED QTR. SAMPLED DATE 3rd 'Sl 27-Aug-S1 4th'Sl 20-0ct-Sl 2nd '82 15-Apr-82 3rd'82 01-Jul-82 4th '82 30-Nov-82 2nd'S3 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd'S4 28-Jun-84 4th '84 14-Nov-84 2nd '85 27-Mar-85 3rd '85 15-Jul-85 4th '85 09-0ct-85 2nd '86 24-Mar-86 3rd '86 10-Jul-86 4th '86 IS-Dee-86 2nd '87 20-Apr-87 3rd '87 OS-Jun-87 4th '87 22-0ec-87 2nd '88 19-Apr-88 3rd '88 28-Jul-88 2nd '89 07-Apr-89 3rd '89 06-Jun-89 4th '89 07-Nav-89 1st '90 17-Apr-90 2nd '90 20-Jun-90 3rd '90 17-0ct-90 1st '91 lO-Apr-91 2nd '91 ll-J un-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 lO-Jun-92 3rd '92 lO-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd'93 12-0ct-93 1st '94 ll-May-94 2nd '94 19-Jul-94 3rd '94 28-Nov-94 1st '95 ll-Apr-95 2nd '95 06-Jul-95 3rd '95 lS-Nov-95 1st '96 23-Apr-96 2nd '96· 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd '97 05-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 OS-Nov-98 2nd '99 15-Apr-99 3rd '99 07-Jul-99 4th '99 02-Dec-99 2nd '00 21-Apr-00 2nd 'oa 22-Jun-OO 4th '00 21-0ec-OO 1st '01 30-Apr-01 2nd '01 14-Jun-Ol Ra·226 Ra·226 VALUE (u(I/Kg) ERROR (u(i/Kg) 2.73E-03 5.0E-05 2.00E-04 1.0E-05 1.04E-04 9.0E-06 2.ooE-05 l.OE-05 2.36E-06 9.5E-07 8.58E-05 1.4E-05 1.19E-04 1.1E-05 9.78E-05 7.0E-06 2.08E-04 1.0E-05 6.05E-04 1.6E-04 1.10E-04 8.0E-06 6.1OE-05 6.0E-06 1.07E-04 6.0E-06 8.86E-04 1.8E-05 6.66E-04 1.8E-05 5.20E-04 1.0E-04 4.10E-04 1.0E-04 1.60E-04 3.0E-05 3.60E-04 5.0E-05 2.60E-04 5.0E-05 3.1OE-05 1.9E-05 6.20E-04 5.0E-05 3.40E-04 3.0E-05 5.1OE-04 6.0E-05 3.60E-04 3.0E-05 1.70E-04 2.0E-05 8.80E-05 1.6E-05 3.ooE-04 3.OE-05 3.10E-04 3.0E-05 5.00E-04 4.0E-05 2.00E-05 8.0E-06 6.50E-06 6.0E-06 1.20E-04 4.0E-05 1.80E-05 1.7E-05 5.20E-05 1.9E-05 5.10E-05 2.3E-05 1.20E-04 1.0E-05 3.73E-05 1.6E-06 2.40E-04 1.5E-05 8.40E-05 6.1E-06 1.90E-05 1.5E-06 1.20E-04 6.8E-06 8.30E-05 3.3E-06 3.60E-05 2.5E-06 3.30E-05 2.3E-06 5.40E-06 3.5E-07 8.90E-06 7.2E-07 <9.20E-05 9.2E-05 < 6.50E-08 6.5E-08 4.20E-05 1.0E-06 6.20E-05 1.0E-06 5.45E-05 1.4E-06 1.10E-04 3.0E-06 3.70E-05 1.0E-06 2.90E-05 1.0E-06 2.30E-06 1.4E-06 2.10E-05 1.0E-06 1.30E-06 4.0E-08 LLD Pb-210 Pb-210 LLD uti/Kg (5.0E-OS) VALUE (u(i/Kg) ERROR (u(I/Kg) u(I/Kg (1.0E-06) 5.0E-OS 7.10E-03 3.0E-04 1.0E-06 5.0E-08 8.30E-04 5.0E-05 1.0E-06 7.0E-06 6.40E-04 5.0E-05 4.0E·05 5.0E-08 2.20E-04 9.0E-05 1.0E·07 1.0E-06 8.00E-05 1.0E-05 1.0E-05 2.OE-08 3.53E-04 1.9E-05 1.0E-05 5.0E-06 1.58E-04 1.3E-05 1.0E-05 2.0E-06 2.16E-03 3.4E-04 3.0E-04 3.0E-09 1.60E-03 7.0E-05 3.0E-08 2.0E-07 2.58E-03 1.1E-04 3.0E-08 3.0E-06 8.63E-04 4.2E-05 3.0E-05 2.0E-06 5.40E-04 5.0E-05 5.0E-05 2.0E-06 3.80E-04 3.OE-05 2.OE-05 2.0E-06 4.40E-03 1.9E-04 3.0E-05 3.0E-06 4.78E-03 2.1E-04 6.0E-05 3.0E-06 1.70E-03 1.0E-04 6.0E-05 5.0E-08 1.60E-03 1.0E-04 1.0E-06 5.0E-08 5.50E-04 4.0E-05 1.0E-06 5.0E-08 1.80E-03 1.0E-04 1.0E-06 5.0E-08 1.90E-03 1.0E-04 1.0E-06 5.0E-08 1.60E-04 4.0E-05 1.0E-06 ... 1.70E-03 1.0E-04 ... ... 7.40E-04 3.0E-05 ... 7.0E-06 1.00E-03 7.0E-05 1.4E-05 4.0E-06 4.80E-04 2.0E-05 2.2E-05 5.0E-08 3.20E-04 2.0E-05 1.0E-06 5.0E-OS 2.90E-04 2.0E-05 1.0E-06 5.0E-06 4.10E-04 2.0E-05 1.0E-06 2.0E-07 4.70E-04 2.0E-05 2.0E-07 5.0E-08 1.50E-03 1.0E-04 1.0E-06 2.0E-06 9.60E-05 1.4E-05 l.OE-05 2.0E-06 1.20E-04 2.0E-05 1.0E-06 3.0E-06 1.21E-03 8.0E-05 2.0E-05 3.0E-06 2.1OE-04 3.0E-05 2.0E-05 3.0E-06 1.70E-05 3.6E-05 2.0E-05 3.0E-06 7.1OE-04 6.0E-05 2.0E-05 3.0E-05 9.80E-04 1.6E-04 2.0E-04 8.4E-08 7.80E-05 7.1E-06 4.2E-07 1.7E-07 2.60E-04 1.3E-05 8.3E-07 1.5E-07 1.20E-04 1.1E-05 7.5E-05 1.4E-07 4.50E-05 4.3E-06 7.2E-07 1.4E-07 1.00E-05 5.8E-06 7.1E-07 1.9E-07 6.80E-05 6.3E-06 1.8E-07 1.6E-07 8.50E-05 5.6E-06 8.4E-07 1.7E-07 4.40E-05 4.8E-06 8.4E-07 1.6E-07 3.20E-05 9.0E-07 7.8E-07 5.4E-07 3.40E-04 6.7E-06 1.1E-07 9.2E-05 <4.60E-04 4.6E-04 4.6E-04 6.5E-08 <3.20E-07 3.2E-07 3.2E-07 1.1E-07 1.70E-04 1.0E-05 5.5E-07 1.0E-07 1.40E-04 7.0E-06 1.0E-07 8.3E-08 9.20E-05 4.0E-06 4.2E-07 2.2E-07 2.80E-05 1.0E-06 1.1E-06 2.4E-07 2.70E-04 1.0E-05 1.2E-06 3.3E-07 2.80E-04 2.0E-05 1.7E-06 3.7E-07 3.30E-04 5.0E-05 1.9E-06 1.5E-07 <7.6E-07 N/A 7.6E-07 1.2E-07 1.80E-06 3.0E-08 5.9E-07 4th '01 17-Dec-Ol 3.70E-OS 7.67E-07 B.30E-OB 6.72E-OS 2.62E-06 6.00E-07 1st '02 07-M.y-02 4.90E-OS 2.40E-06 7.60E-07 l.2BE-04 S.61E-06 l.OOE-OS 2nd '02 07-Jul-02 B.BBE-OS 4.32E-06 7.60E-07 B.33E-OS 4.32E-06 l.OOE-OS 4th '02 lS-Oec-02 l.SOE-04 6.2E-06 7.60E-07 3.16E-04 l.OlE-OS l.OE-OS 1st '03 21-Mar-03 S.OOE-OS 3.4E-06 2.71E-06 <4.1e-6 4.20E-06 2nd '03 1O-Jun-03 S.60E-OS 2.0E-06 4.lOE-07 l.BBE-04 S.14E-06 B.2E-OB 4th '03 20-Nov-03 3.20E-04 B.2E-06 l.70E-07 4.B9E-04 l.2SE-OS B.3E-07 1st '04 OB-Apr-04 6.29E-OS 4.1E-06 2.00E-07 l.94E-OS 4.00E-06 l.OE-06 2nd '04 12-Jun-04 6.51E-OS 3.4E-06 l.30E-07 l.8lE-OS 3.90E-06 6.5E-07 4th '04 30-Nov-04 7.50E-OS 4.6E-06 2.0E-OB 4,4SE-04 1,40E-OS 3.0E-07 1st '05 21-Apr-OS 4.90E-OS 2.70E-06 l.30E-07 l.27E-04 4.BOE-06 6.S0E-07 2nd 'OS 13-Jun-05 2.30E-OS 2.10E-06 1.50E-07 4.70E-OS S.10E-06 7.60E-07 4th 'OS lO-Nov-OS 7.40E-OS 3.50E-06 l.20E-10 2,40E-06 B.10E-OB S.BOE-10 1st '06 03-Apr-06 l.00E-04 6.00E-06 S.OOE-OB 6.54E-04 l.SOE-OS 1.00E-06 2nd '06 16-Jun-06 9.50E-OS S.90E-06 S.OOE-OB 4.4BE-04 lAOE-OS 1.00E-06 4th '06 28-Nov-06 B.13E-OS 4.10E-06 2.20E-07 3.2SE-04 1.12E-06 l.OOE-OS 1st '07 30-Mar-07 4.30E-OS 2.60E-06 l.70E-07 2.64E-04 7.20E-06 B.60E-07 2nd '07 I-Jun-07 S.lOE-OS 3.20E-06 2.30E-07 S.30E-04 1,40E-06 l.20E-06 4th '07 23-Nov-07 7.30E-OS 6.6E-06 S.OE-OB 7.00E-04 2.20E-OS 1.10E-06 1st '08 22-Apr-OB 2.BE-06 2.BE-06 7.20E-07 4.40E-04 2.0E-OS l.OE-06 2nd 'OB 18-Jun-08 3.2E-06 3.3E-06 l.BOE-06 1,40E-04 BE-OS S.5E-OS 4th 'OB 12-0ec-08 7.3E-OS 3.2E-06 7,40E-07 4.40E-04 2.SE-OS 3.2E-OS 1st '09 2B-Apr-09 S.3E-OS 3.6E-06 1.10E-06 l.90E-04 l.SE-OS 2.2E-OS 2nd '09 17-Jun-09 2.3E-OS l.6E-OS S.2E-07 4.30E-OS 1.00E-OS l.7E-OS 4th '09 18-0ec-09 S.50E-OS 3.50E-06 3.0E-04 1.10E-OS 1st '10 13-M.y-lO l.9E-04 6.10E-06 9.40E-07 S.lE-04 2.40E-OS 3.lOE-OS 2nd '10 18-Jun-l0 2.3E-OS 2.00E-06 7.70E-07 B.3E-OS l.BOE-OS 2.90E-OS 4TH '10 20-0ec-IO B.6E-06 9.10E-07 3.90E-07 l.lE-07 6.BOE-07 1.10E-06 "'2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period WHITE MESA Mill FORAGE RADIO NUClIDE DATA SOUTHWEST OF Mill SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd '82 15-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nav-82 2nd '83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-84 2nd '85 27-Mar-85 3rd '85 15-Jul-85 4th '85 09-0ct-85 2nd '86 24-Mar-B6 3rd '86 10-Jul-86 4th '86 IS-Dee-86 2nd '87 20-Apr-87 3rd'87 05-Jun-87 4th '87 22-Dec-87 2nd '88 19-Apr-88 3rd '88 28-Jul-88 2nd '89 07-Apr-89 3rd '89 06-Jun-89 4th '89 OJ-Nav-89 1st '90 17-Apr-90 2nd 'gO 20-Jun-90 3rd'90 17-0ct-90 1st '91 IO-Apr-91 2nd '91 11-Jun-91 3rd'91 20-Nov-91 1st '92 22-Apr-92 2nd '92 10-Jun-92 3rd'92 10-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd'93 12-0ct-93 1st '94 ll-May-94 2nd '94 19-Jul-94 3rd '94 28-Nov-94 1st '95 U-Apr-95 2nd '95 06-Jul-95 3rd '95 15-Nov-95 1st '96 23-Apr-96 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd '97 05-5ep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 05-Nov-98 2nd '99 15-Apr-99 3rd '99 07-Jul-99 4th '99 02-0ec-99 2nd 'oa 21-Apr-00 2nd '00 22-Jun-OO 4th '00 21-0ec-OO 1st '01 30-Apr-01 2nd '01 14-Jun-01 Ra-226 Raw 226 VALUE (uCi/Kg) ERROR (uCi/Kg) 9.50E-04 2.0E-05 3.00E-05 3.0E-06 1.37E-05 3.0E-06 3.40E-04 2.OE-05 1.75E-05 3.0E-06 7.13E-04 7.3E-05 5.39E-05 4.5E-06 6.40E-05 7.0E-06 8.27E-05 6.3E-06 2.72E-04 1.5E-04 4.73E-04 1.6E-07 6.60E-05 7.0E-06 2.83E-04 2.0E-05 1.57E-04 l.OE-05 3.78E-04 l.OE-05 2.60E-04 2.OE-05 4.1OE-04 7.0E-05 2.90E-04 4.0E-05 1.80E-04 3.0E-05 2.30E-04 5.0E-05 1.50E-04 3.0E-05 3.10E-04 4.0E-05 1.30E-04 2.OE-05 4.30E-04 5.0E-05 2.50E-04 3.0E-05 1.10E-04 2.0E-05 6.1OE-05 1.4E-05 3.40E-05 1.1E-05 8.00E-05 6.0E-06 6.50E-05 1.4E-05 1.60E-05 7.0E-06 1.90E-05 l.OE-05 1.60E-05 1.8E-05 2.60E-05 2.0E-05 3.00E-05 1.4E-05 3.1OE-05 1.6E-05 2.00E-05 5.0E-06 1.75E-05 1.7E-06 1.00E-04 9.0E-06 1.70E-05 1.5E-06 6.40E-06 6.0E-07 2.30E-05 2.2E-06 4.20E-05 2.2E-06 2.1OE-05 2.0E-06 5.50E-06 4.2E-07 5.30E-06 3.2E-07 2.50E-05 9.5E-07 <7.90E-OS 7.9E-05 3.60E-07 1.4E-07 4.30E-05 1.0E-06 2.40E-05 1.0E-06 2.23E-05 8.6E-07 1.50E-04 3.0E-06 1.00E-04 2.0E-06 1.30E-06 1.0E-07 1.20E-06 9.0E-07 1.80E-06 1.0E-07 2.60E-06 2.0E-07 llD Pb-210 Pb-210 llD uCi/Kg (5.0E-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (1.0E-06) 5.0E-08 1.50E-04 1.0E-05 1.0E-06 5.0E-08 1.50E-04 2.0E-05 1.0E-06 3.0E-06 3.80E-04 4.0E-05 4.0E-05 5.0E-08 3.68E-03 2.7E-04 1.0E-07 2.0E-06 7.92E-04 4.0E-06 2.0E-05 9.0E-08 2.51E-03 3.0E-04 3.0E-04 2.0E-06 6.88E-04 4.3E-05 4.0E-05 4.0E-06 1.20E-03 1.0E-04 4.0E-05 3.0E-09 1.80E-03 1.0E-04 9.0E-08 2.0E-07 4.70E-03 7.2E-04 3.0E-07 3.0E-06 7.07E-04 3.6E-05 3.0E-05 4.0E-06 4.90E-04 3.0E-05 3.0E-05 7.0E-06 1.50E-03 1.0E-04 7.0E-05 4.0E-06 4.14E-03 1.8E-04 3.0E-05 2.0E-06 1.65E-02 7.0E-04 1.0E-04 2.0E-06 1.70E-03 1.0E-04 1.0E-04 5.0E-08 2.20E-03 1.0E-04 1.0E-06 5.0E-08 7.50E-04 5.0E-05 1.0E-06 5.0E-08 2.40E-03 1.0E-04 1.0E-06 5.0E-08 2.90E-03 1.0E-04 1.0E-06 5.0E-08 4.30E-03 2.0E-04 1.0E-06 ... 4.20E-03 1.0E-04 ... ... 1.50E-03 1.0E-04 ... 1.4E-05 3.50E-03 1.4E-04 2.7E-05 5.0E-06 2.39E-03 5.0E-05 2.5E-05 5.0E-08 6.60E-04 3.0E-05 1.0E-06 5.0E-08 6.10E-04 3.0E-05 1.0E-06 5.0E-06 2.20E-04 1.0E-05 1.0E-06 2.0E-07 1.20E-04 1.0E-05 2.0E-07 5.0E-08 9.10E-04 5.0E-05 1.0E-06 2.0E-06 3.20E-04 2.0E-05 1.0E-05 2.0E-07 2.20E-04 2.0E-05 1.0E-06 3.0E-06 7.60E-04 6.0E-05 2.0E-05 3.0E-06 3.40E-04 3.0E-05 2.0E-05 3.0E-06 O.OOE+OO 3.0E-05 2.OE-05 3.0E-06 4.20E-04 6.0E-05 2.0E-05 3.0E-05 3.90E-04 8.0E-05 2.0E-04 7.6E-08 1.30E-04 7.8E-06 3.8E-07 1.5E-07 2.60E-04 1.2E-05 7.4E-07 1.6E-07 1.60E-04 1.5E-05 8.1E-07 1.4E-07 4.40E-05 4.2E-06 7.0E-07 1.7E-07 6.60E-05 9.6E-06 8.3E-07 1.7E-07 1.00E-04 6.7E-06 1.8E-07 1.6E-07 1.90E-04 7.3E-06 8.2E-07 1.4E-07 3.30E-05 3.9E-06 7.0E-07 1.3E-07 1.90E-05 6.9E-07 6.3E-07 5.9E-07 1.30E-04 4.7E-06 1.2E-07 7.9E-05 <3.90E-04 3.9E-04 3.9E-04 3.3E-08 <1.7E-07 1.7E-07 1. 7E-07 7.6E-08 2.50E-04 1.0E-05 3.8E-07 1.2E-07 1.70E-04 8.0E-06 6.2E-07 1.2E-07 2.30E-04 7.0E-06 5.9E-07 2.0E-07 1.70E-05 1.0E-06 1.0E-06 1.2E-07 1.10E-04 7.0E-06 6.1E-07 2.4E-07 2.00E-04 l.OE-05 1.2E-06 2.4E-07 1.20E-04 3.0E-05 1.2E-06 1.7E-07 <8.3E-07 N/A 8.3E-07 9.9E-08 1.10E-06 2.0E-08 5.0E-07 4th '01 17·0ec-01 2.63E-06 4.6E-Os L2E-07 9.40E-Os 3.7E-06 6.0E-07 1st '02 07-M,y-02 3.50E-Os 2.2E-06 7.6E-07 l.36E-04 s.6E-06 LOE-Os 2nd '02 07-Jul-02 4.02E-Os 2.3E-06 7.6E-07 7.04E-Os 4.1E-06 LOE-Os 4th '02 ls-Doc-02 B.1OE-Os 3.9E-06 7.6E-07 2.B7E-04 B.sE-06 LOE-Os 1st '03 21-Mar-03 3.70E-Os 2.6E-06 2.4E-06 2.69E-Os 2.0E-06 3.7E-06 2nd '03 10-Jun-03 l.30E-Os LOE-06 s.2E-07 <l.ODE-07 LOE-07 4th '03 20-Nov-03 L 60E-04 l.3E-Os l.2E-07 1.42E-04 6.4E-06 s.9E-07 1st '04 OB-Apr-04 1.40E-04 7.7E-06 l.lE-07 6.10E-06 2.7E-06 s.5E-07 2nd '04 12-Jun-04 6.s1E-Os 3.2E-06 1.5E-07 s.27E-Os 4.9E-06 7.6E-07 4th '04 30-Nov-04 B.40E-Os s.7E-06 3.0E-OB 3.39E-04 L6E-Os 3.0E-07 1st '05 21-Apr-OS L70E-Os L6E-06 l.3E-07 4.s0E-Os 3.sE-06 6.5E-07 2nd '05 13-Jun-05 LsOE-Os L6E-06 1.4E-07 7.00E-Os s.lE-06 6.9E-07 4th '05 IO-Nav-OS 3.BOE-Os 2.1E-06 B.6E-1O l.20E-06 4.BE-OB 4.3E-1O 1st '06 03-Apr-06 LOOE-04 6.0E-06 s.OE-OB 3.30E-04 L1E-Os 1.0E-06 2nd '06 16-Jun-06 3.40E-Os 2.5E-06 s.OE-OB l.37E-04 6.0E-06 LOE-06 4th '06 28-Nav-06 7.31E-Os 3.20E-06 L60E-07 2.9BE-04 B.50E-06 B.20E-07 1st '07 30-Mar-C7 3.00E-Os 2.20E-06 L70E-07 3.20E-04 7.90E-06 B.40E-07 2nd '07 I-Jun-07 1.10E-04 4.60E-06 2.3-07 3.20E-04 1.10E-Os 1.10E-06 4th '07 23-Nov-07 s.60E-Os s.20E-06 s.OOE-OB 6.40E-04 L90E-Os LOOE-06 1st '08 22-Apr-OB 3.20E-Os 2.30E-06 7.20E-07 2.30E-04 1.50E-Os LOOE-06 2nd 'OB 18-Jun-08 l.2sE-Os 2.20E-06 LBOE-06 s.OOE-Os 3.00E-Os 4.BOE-03 4th 'OB 12-0ec-08 1st '09 2B-Apr-09 2.60E-Os 2.90E-06 L40E-06 3.70E-Os LsOE-06 2.50E-Os 2nd '09 17-Jun-09 2.40E-Os L40E-06 3.90E-07 3.50E-Os 7.90E-06 1.30E-Os 4th '09 18-Dec-09 3.1E-Os 2.30E-06 2.1E-04 B.40E-06 1st '10 13-M,y-l0 2.0E-Os 2.10E-06 9.40E-07 s.6E-Os LsOE-Os 2.40E-Os 2nd '10 18-Jun-l0 l.lE-Os l.30E-06 6.60E-07 7.BE-Os L60E-Os 2.s0E-Os 4th '10 20-Dec-IO 6.7E-06 9.1OE-07 4.BOE-07 B.OE-07 7.90E-07 l.30E-06 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period EN:RGY _1\<:10111\1 OI~ll_~ www.er.ergylab.com AM/ftJ&II Ealkt s.c. 1m H.I.na, MT 871-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-0515 GiII.H., WY 866-686-7175 ' Rapid City, SO 888-672-1225 ' Coli.!. Station, IX 881-690-2218 February 09, 201 1 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: Cl 0120777 Project Name: Late Fall Vegetation ANALYTICAL SUMMARY REPORT Energy Laboratories, Inc. Casper WY received the following 3 samples for Denison Mines USA Corp on 12/22/2010 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test Cl0120777-001 North East 12/20/1014:4012/22/10 Vegetation Digestion, Radiochemistry Lead 210 Radium 226 Cl0120777-002 North West 12/20/1013:1012/22/10 Vegetation Same As Above Cl0120777-003 South West 12/20/10 1 0 :30 12/22/10 Vegetation Same As Above This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: ~~ . Technical Diredor Digitally signed by Steve Carlston Date: 2011.02.0911:12:25 -07 :00 Page 1 of 9 www.energylab.com AIu/JfJcM lrcMJH&. SMu '151 Helena, MT 871-412-l1111 • Billin!_, NT 800-135-4-489 • Cosper, WI 888-235-0515 GIII.tt. WI 866-186-1115 ' R. Id C ,SD 188-612-1225 ' Coli •• SI.tlon TJl 88I-690-2218 CLIENT: Denison Mines USA Corp Project: Lale Fall Vegelalion Sample Delivery Group: Cl01 20777 ORIGINAL SAMPLE SUBMITTAL(S) All original sample submitlals have been relurned with Ihe data package. SAMPLE TEMPERATURE COMPLIANCE: 4'C (±2'C) Report Date: 02/09/11 CASE NARRATIVE Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking waler melhod for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avo id excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Dala for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Arcclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYS IS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize ils branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gilletle, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. - Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC : E87641 , Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Vi rginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The resu lts of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections conlained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the clie nt may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. Page 2 of 9 EN:RGY /\1 OIU\IClIll ~ www.energylab.com AIIIIftiuI lrulllll&. SIIu ,m Helena, MT 877·472·0711 • Billings, MT 800·735·4489 • Casper, WI 888·235·0515 Gillette, WI 866·186·7175 • Rapid City, SD 888·612·1225 • Colleg. Station, n 888·69D·2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab lD: Denison Mines USA Corp Late Fall Vegetation Cl0120777·001 Client Sample ID: North East Analyses RADIONUCLIDES • TOTAL Lead 210 Lead 210 precision (±) Lead 210 MDC Lead 210 allu Lead 210 precision (±) allu Lead 210 MDC altu Radium 226 Radium 226 precision (±) Radium 226 MDC Radium 226 altu Radium 226 altu precision (±) Radium 226 allu MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality conlrol limit. Result 1.0E-05 1.5E·06 2.3E·06 10.2 1.5 2.3 2.3E-05 1.7E·06 5.2E·07 23.3 1.7 0.52 Units uCi/kg uCi/kg uCi/kg pCi/kg pCl/kg pCilkg uCi/kg uCi/kg uCi/kg pCilkg pCilkg pCilkg MDC -Minimum detectable concentration Qualifiers RL Report Date: 02/09/11 Coliection Date: 12/20/1014:40 DateRecelved: 12/22/10 Matrix: Vegetation MCU aCL Method Analysis Date 1 By E909.0 01127/11 21 :56 1 eli-cs E909.0 01127/11 21 :56 1 eti-cs E909.0 01127/11 21 :56 1 eti-cs E909.0 01127/11 21 :56 1 eli-cs E909.0 01127/11 21 :56 1 eli-cs E909.0 01127/11 21 :56 1 eli-cs E903.0 01119/11 10:41 Itrs E903.0 01/19/11 10:411trs E903.0 01/19/11 10:411trs E903.0 01/19/1110:411trs E903.0 01/19/1110:41/1rs E903.0 01119/11 10:411trs MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 3 of 9 EI\ERGY 1\1 ,)!I;qCI~1I • WNW.energylab.com AIlIITbI ExuIIItIcI SIIu 1m Helena, MT 871-412-0111 • Billin!., MT 800-735-4489 • Cuper, WY 881-235-0515 Gillette, WY 866-68li-7175 • Rapid C"y, SD 188-672-1225 • CoHe!e SI.tion, TJl UI-69D-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp Late Fall Vegetation Cl0120777-002 Client Sample 10: North West Analyses RADIONUCLIDES -TOTAL Lead 210 Lead 210 precision (±) Lead 210 MDC Lead 210 altu Lead 210 precision (±) altu Lead 210 MDe altu Radium 226 Radium 226 precision (±) Radium 226 MDe Radium 226 altu Radium 226 altu precision (±) Radium 226 attu MDC Report Definitions: Rl . Analyte reporting limit. QCl . Quality control limit. Result -1.IE-07 6.8E-07 1.1 E-06 -0.11 0.68 1.1 8.6E·06 9.1E·07 3.9E·07 8.6 0.91 0.39 Units uei/kg uei/kg uei/kg pCi/kg pCi/kg pCi/kg uei/kg uei/kg uei/kg pCi/kg pCi/kg pCi/kg MDC . Minimum detectable concentration Report Date: 02/09/11 Collection Date: 12/20/1013:10 DateReceived: 12/22/10 Matrix: Vegetation MCL! Qualifiers RL QCL Method Analysis Date I By U E909.0 02104/11 01 :21 I eli-cs E909.0 02104/11 01:21 I eli-cs E909.0 02/04/11 01 :21 I eJi-cs U E909.0 02104/11 01 :21 1 eli·cs E909.0 02104/11 01 :21 1 eli·cs E909.0 02104/11 01 :21 I eli-cs E903.0 01119/11 10:41/1rs E903.0 01/19/1110:41/trs E903.0 01/19/1110:41 /1rs E903.0 01l19/1110:41/1rs E903.0 01l19/1110:41 /1rs E903.0 01/19/1110:41/1rs MCl . Maximum contaminant level. ND -Not detected at the reporting limit. U • Not detected at minimum detectable concentration Page 4 of 9 EN:RGY ,/\!IOJIAIC11<i! " YtWW.energylab.com AIuIytJcM ExullHct Sbru rill Helena, MT 871-412-0111 • Billin!', MT 800-131-4489 • C .. per, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 188-612-1225 • Colle!. Station, IX 881-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp Late Fall Vegetation C10120?77-003 Client Sample 10: South West Analyses RADIONUCLIDES -TOTAL lead 210 Lead 210 precision (±) lead 210 MDC Lead 210 altu Lead 210 precision (±) altu Lead 210 MOe altu Radium 226 Radium 226 preCision (±) Radium 226 MDe Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOe Report Definitions: AL -Analyte reporting limit. QCL -Quality conlrollimit. Result 8.0E-0? 7.9E-07 1.3E-06 0.80 0.79 1.3 6.7E·06 9.1 E-07 4.8E-07 6.7 0.91 0.48 MDC -Minimum detectable concentration Units uGilkg uCilkg uCi/kg pCilkg pCi/kg pCi/kg uCilkg uCilkg uCi/kg pCi/kg pCi/kg pCi/kg Report Date: 02109111 Collection Date: 12120110 10:30 DateRecelved: 12122110 Matrix: Vegetation MCll Qualifiers Rl QCl Method Analysis Date I By U E909.0 02104/11 07:54 1 eli-cs E909.0 02104111 07:54 1 eli-es E909.0 02104/11 07:54 / eli-cs U E909.0 02104/11 07:54 I eli-cs E909.0 02104/11 07:54 I eli-cs E909.0 02/04/11 07:54/ eli-cs E903.0 01l19/1110:41 /trs E903.0 01l19/1110:41 /Irs E903.0 01l19/1110:41 /trs E903.0 01/19/11 10:41 /trs E903.0 01/19/1110:41 /trs E903.0 01/19/1110:41 /trs MCl . Maximum contaminant level. ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 5 of 9 EN:RGY /\)) lIU\I(,1I1> '> WiI'W.energylab.com AIuIytIcM ExuIIHcI Sba ,m H,len., MY 817-472-0711 • Billing., MT 800-735-4489 • Casper, WY 888-235-0515 GiII.tt., WY 866-&86-1175 • R.pid City, so 888-672-1225 • College StaU"" 1l( 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Cllen1: Denison Mines USA Corp Project: Lale Fall Vegetation Analyte Method: E903.0 Sample 10: Cl0120777-001AOUP Radium 226 Radium 226 precision (±) Radium 226 MOe Sample 10: C10120777-003AMS Radium 226 Sample 10: LCS-28757 Radium 226 Sample 10: MB-28757 Radium 226 Radium 226 precision (±) Radium 226 MOe Qualifiers: RL . Analyle reporting limit. Count Result Units 3 Sample Duplicate 1.9E-05 uCi/kg 1.5E-06 4.7E-07 uCi/kg uCi/kg Sample Matrix Spike 2.4E-05 uCi/kg Laboratory Control Sample 1.5E-05 uCi/kg 3 Method Blank 3E-07 2E-07 4E-07 uCi/kg uCi/kg uCiJkg MOe· Minimum delectable concentration Report Dale: 02/09/11 Work Order: Cl0120777 RL %REC Low Limit High Limit RPO RPOLlmlt Qual 11 1 124 Run: BERTHOLD 770-1_110113A 18 Run: BERTHOLD 770-1_110113A 70 130 Run: BERTHOLD 770·1_1101 13A 70 130 Run BERTHOLD770·1_110113A NO . Not detected at the reporting limit. Batch: 28757 01 /19/11 10:41 24.9 01 /19/11 10:41 01/19/1110:41 01/1911 t 10:41 U U -Not detected at minimum detectable concentration Page 6 of 9 EN:RGY "1\1 JOllA 1 UI~ll ::. www.energylab.com AMfJtIc6f ExUUMJ&. smc. 1m Helena, MT 877-472-11711 • 8imngs, MT 800-735-4489 • Casper, WI 888-235-0515 Gillette, WI 866-686-7175 • R.pid CHy, SO 888-612-1225 • College SI.lioo, TX 888-680-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Late Fall Vegetation Analyte Count Result Units Method: E909.0 SamplelD: Cl0120777-001A Lead 210 Sample ID: Cl0120777-001 A Lead 210 Sample lD: LCS-13117 /28757 Lead 210 SamplelD: MB-13117 I 28757 Lead 210 Lead 210 precision (±) Lead 210 MDC Qualifiers: RL -Analyle reporting limit. Sample Matrix Spike Duplicate 0.00025 uCi/kg Sample Matrix Spike 0.00025 uCVkg Laboratory Control Sample 0.00028 uCi/kg 3 Method Blank 1 E·06 uCVkg 5E-06 uCi/kg 9E-06 uCi/kg MDe -Minimum detectable concentration RL Report Date: 02 /09/11 Work Order: C 1 0120777 %REC low limit High Limit RPD RPDLlmlt Qual Balch: T_13117 Run: SUB-T38688 01128/1102:19 86 70 130 2.8 15.8 Run: SUB-T38688 01128/11 00:08 92 70 130 Run: SUB-T38688 01 /27/11 19:45 74 70 130 Run: SUB-T38688 01 /27/1117:33 U ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 70f9 EN:RGY L,\UOf,/\lCIIH , Yl'ww.energylab.com """""ExuIJHu_ lISt He~na, MT B7J-472-0711 • Billing., MT 800-135-4489 . Ces,,,, WI 881-235-0515 Gillette, WI 866-686-11J5 • Rapid City, SO 888-612-1225 • ColI.g. Station, IX 881-680-2218 Workorder Receipt Checklist Denison Mines USA Corp C10120777 Login completed by: Corinne Wagner Reviewed by: BL2000lkschroeder Reviewed Date: 12/29/2 010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerlTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 NINe Yes 0 Yes 0 Date Received: 12/22/2010 Received by: ha No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Carrier name: Next Day Air Not Present 0 Not Present 0 Not Present 0 No VOA vials submitted III Not Applicable 0 Page 8 019 1i ..... irlCi? Chain of Custody and Analytical Request Record Ritil.U&".Zrlf:i' . . . PLEASE PRINT Provide as much ,"formation as ossible. Page __ of __ compan~e:. " Proiect Na:: PWS. Permit. Etc" Sample Origin \ :;>""'.,c,J ('I/'T"e;, le-4 f",,!/ ~,h..Ho..v State fA "I Yes ~ No D I Report Mail Address;" I' CJ:ct Name: . 'Phone/Fax: Email: ft.. 0 D~ &Jf j) i<L_J.· -IA,:'" INS// P,N f1,./"",~ tr-,r-'Z2ZI Invoice Address: I I invoide Contact & Phone: ~~~ ~ Special Report/Formats: DDW D POTWMlWTP D State: ___ _ o Other: ___ _ SAMPLE IUt:NIIHl;AIIUN ~ ~ 1 ~ '\'7@!]§ 1Alrn@(l!J~00) ~o (l)1? ~m;gOI43 B>~ ~ro D EDD/EDT(Electronic Data) §;~ ~ ~ Fonnat: ~ «ci5I.Q,~ D 0 ~ID c LEVEL IV ~ iii 2 c 'c o.RlOO J 0).: Q5;: <' zo:ct:1ara ...... E >1 ........ 3l t'\ ~ D NELAC ~I'iii • ] M4TRIlC c.. (Name, Location, Interval, etc.) Date Time .. 0 ~ R UJ t:. :r: "C t) e <l: e I U I-'" l-e <l: " f-I 5 UJ "E UJ '" (/) "C e co U5 I H Sampler: (Please Print) I ~"w AL~ Order: Contact ELI prior to RUSH sample submtttal for charges and scheduling -See Instruction Page Comments: Order: ISh' .... bY' , ("\ d),. Q:2~~~1 I CoOler lO(s): toh {eceiPtff !l0 °c I anI,.: Y ~ cU';:'o:" Soag, M OnCoo~r N Intact N ISignature -N Match ·1JC!1!;rJL£A~-r.'S71~~/I.2·.2CJIc1 /I~'iO /I-V /)(IX II I I I I I II I _~ l'Atoau-//Ie::;, q331q b ;p'}Oi/3Io /l-viXl )(1 1 1 1-1 -I 1 1 1 1 ~ I :>~ 0k~1'S~ ~2a?IO I 105-0 I /-V IXF I I I I I I I I I I I i J I: I I ll i ll r II 111 I I i ~ r: I I I I I I I I I I I I I I I ffOt:1D77 I " FJl I Custody R"""""" by (p,'~): -D'lefT'me: Sign"",,: Record Received by (prir(): Oat ime: SignalUre: ~~STbe~------------------~-------4~,~y ~.~,,~o~~-\~.~~~.------~==------~ _190 ed Sample Disposal: ReturnloClienl: LabDisposal:1.J;.k\C) ..M..O_,j:~~~g£~~1. In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. \roc:it our w~h site at www.eneravlab.com for additional information. downloadable fee schedule, forms. and links. ATTACHMENT G STACK SAMPLE LABORATORY RESULTS Prepared for: THIRD QUARTER RADIONUCLIDE EMISSIONS TEST CONDUCTED AT DENISON MINES CORPORA nON NORTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE BLANDING, UTAH August 24-25, 2010 by: TETCO 391 East 620 South American Fork, UT 84003 Phone (801) 492-9106 Fax (801) 492-9107 fax Denison Mines Corporation 6425 S Hwy 91 Blanding, Utah 84511 Date of Report: October 23, 2010 CERTIFICATION OF REPORT INTEGRITY Technical Emissions Testing Company (TETCO) certifies that this report represents the truth as well as ca n be derived by the methods employed. Every effort was made to obtain accurate and representative data and to comply with procedures set fort h in the Federal Register. " n II,. Mike McNamara Reviewer:.-----'¥'--"l.1IM--'-/f~ __ Date:._-"-'..O-\...(_'L--"--)..,;",I-'..I"""O'--_____ _ Dean A. Kitchen Reviewer: _____ ~/fJ::;""-''''''A/''''''-'''a'''-.<~'__'''''''__=_ __ Date: ________ w/t/"'-----..<h..!<r_-(wC...,I'----_ ii TABLE OF CONTENTS Introduction Test Purpose ............................................................ 1 Test Location and Type of Process .......................................... 1 Test Dates ............................................................. 1 Pollutants Tested and Methods Applied ...................................... 1 Test Participants ......................................................... 2 Deviations From EPA Methods ............................................. 2 Quality Assurance ....................................................... 2 Summary of Results Emission Results ........................................................ 3 Process Data ............................................................ 3 Description of Collected Samples ........................................... 3 Discussion of Errors or Irregularities ......................................... 3 Percent Isokinetics ....................................................... 4 Source Operation Process Control Devices Operation .......................................... 5 Process Representativeness ................................................ 5 Sampling and Analysis Procedures Sampling Port Location ................................................... 6 Sampling Point Location ..................................•..........•.... 6 Sampling Train Description ................................................ 6 Sampling and Analytical Procedures ......................................... 7 Quality Assurance ....................................................... 7 Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence iii LIST OF TABLES Table I Measured Radionuclide Emissions .......................................... 3 II Percent Isokinetics ....................................................... 4 III Sampling Point Location .................................................. 6 IV Complete Results, North Yellow Cake Scrubber ...................... Appendix A V Complete Results, Yellow Cake Dryer Baghouse ...................... Appendix A LIST OF FIGURES Figure 1 Facility Schematic Representation North Yellow Cake Scrubber .......... Appendix D 2 Facility Schematic Representation Yellow Cake Dryer Baghouse ......... Appendix D 3 Schematic of Method 511 14 Sampling Train . . . . . . . . . . . . . . . . . . . . . . . . . . Appendix E iv INTRODUCTION Test Purpose This test project was conducted to detennine the total radionuclide emissions from the North Yellow Cake Scrubber and the Yellow Cake Dryer Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dscl). These tests were for U-Nat only. Test Location and Type of Process Denison Mines (USA) Corporation is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Dryer Baghouse. The Packaging enclosure also discharges into the Dryer Baghouse. The North Yellow Cake (NYC) dryer was the only operating dryer at the time of the test. The South Yellow Cake Dryer is currently not operational. The Grizzly Baghouse serve as the main dust control device for the raw ore unloading and conveying to the processing building. Stack schematics are shown as Figures I and 2 in Appendix D. Test Dates One test run was completed on the NYC Dryer August 24, 2010 and one run on August 251h One run was completed on the Dryer Baghouse August 24, 20 I O. Pollutants Tested and Methods Applied The tests were a determination of radionuclide emissions in accordance with EPA Method 5/1 14. Test run filters and front wash residues were sent to Test America located in Richland, Washington for radionuclide analysis. Test Participants Test Facility State Agency TETCO Ryan Palmer None Doug Olsen Kawai McNamara Deviations From EPA Methods None Quality Assurance Mike McNamara Testing procedures and sample recovery techniques were according to those outlined in the Federal Register and the Quality Assurance Handbookfor Air Pollution Measurement Systems. 2 SUMMARY OF RESULTS Emission Results Table I presents the findings of the test in Curies per dry standard cubic foot. Tables IV -VI in Appendix A have more detailed information. Table I. Measured Radionuclide Emissions North Yellow Cake Run # Scrubber pCi/dscf pCi/hr 1.974E+02 l.512E +07 2 2.55 1 E+02 1.912E+07 AVE 2.263[+02 1.712[+07 Process Data Yellow Cake Dryer Baghouse pCi/dscf pCi/hr 3.885E+00 4.835E+06 t:o. .' U '_ -_ _ . 3.885[+00 4.835[+06 The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow, pressure drop readings (t.p) were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (t.p) were recorded and are found on the test run sheets. Production data will be submitted by Denison Mines. Description of Collected Samples The test filters for the North Yellow Cake Scrubber were heavily covered with a white or pinkish white colored particulate. The front washes were clear in appearance. The test filters for the Yellow Cake Dryer Baghouse were lightly colored with a tan colored particulate. The front wash was clear in appearance. Discussion of Errors or Irregularities None 3 Percent lsokinetic Sampling Each of the tests were isokinetic within the ± I 0% of 100% criterion specified in the Federal Register. They also meet the Utah State Department of Environmental Quality, Division of Air Quality specification of isokinetic sampling point by point. Isokinetic values for each test run are presented in Table II. Run # I 2 North Yellow Cake Yellow Cake Dryer Scrubber 102 103 4 96 SOURCE OPERA nON Process Control Devices Operation All process control devices were operated nonnally. Recorded scrubber water flow, pressure and baghouse ~p readings were recorded and are found on the test run sheets or in Appendix D. Process Representativeness The facility was operated nonnally. Production data was retained by Denison Mines. 5 SAMPLING AND ANALYSIS PROCEDURES Sampling Port Location The inside diameter of the North Yellow Cake Scrubber stack is 18.0 inches. The two, four-inch diameter sample port are located 6.3 diameters (9.5 feet) downstream from the last disturbance and 6.3 diameters (9.5 feet) upstream from the next disturbance. Figure I in Appendix D is a schematic of the stack. The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-i nch diameter sample ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 2 in Appendix D. Sampling Point Location Table III shows the distance of each sampling point from the inside wall according to EPA Method I. Each point is marked and identified with a wrapping of glass tape and numbered. These points are determined by measuring the distance from the inside wall. Di stance (inches) from Inside Wall Sample Point I 0.58 0.70 2 1.89 2.34 3 3.49 4.74 4 5.81 11.26 5 12.19 13 .66 6 14.51 15.30 7 Sampling Train Description To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-5/114 were followed. All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent interference of the sampled gas and particulate. 6 The stack analyzers used to conduct Methods 1-51114 are constructed to meet the specifications outlined in the CFR. The temperature sensors are K-type thermocouples. Heater, vacuum and pitot line connections have been designed to be interchangeable with all units used by the tester. A 316 stainless steel probe liner was used for the tests. Figure 4 in Appendix E is a sketch of the Methods 51114 sampling train. Sample boxes were prepared for testing by following the prescribed procedures outlined in Methods 5/114. Sampling and Analytical Procedures All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 51114. Quality Assurance All equipment set-up, sampling procedures, sample recovery and equipment calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbookfor Air Pollution Measurement Systems. 7 APPENDIX A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence 8 APPENDIX A Table IV Complete Results, North Yellow Cake Scrubber Table V Complete Results, Yellow Cake Dryer Baghouse Nomenclature Sample Equations A TABLE IV NYC Scrubber COMPLETE RESULTS DENISON MINES CORPORATION, BLANDING, UTAH NORTH YELLOWCAKE SCRUBBER EXHAUST Symbol Descri(?:tion Dimensions Run #1 Run #2 Date 8/24110 8125110 Filter # 5601 5607 Begin Time Test Began 8:15 8:09 End Time Test Ended 16:46 16:36 Pbm Meter Barometric Pressure In. Hg. Abs 24.60 24.65 61-1 Orifice Pressure Drop In. H10 1.454 1.417 Y MeterCalibration Y FaClor dilnensionless 1.000 1.000 Vm Volume Gas Sampled.·Meter Conditions " 364.311 354.674 Tm Avg McterTemperalure 'F 105.2 101.4 -.J6P Sq Root Velocity 1·lead Root In. H2O 0.2823 0.2785 Wtwc Weight Water Collected Grams 1022.0 1011.2 T, Duration of Test Minutes 480 480 Co Pitot Tube Coefficient Dimensionless 0.84 0.84 D, Nozzle Diameter Inches 0.3813 0.3813 CO, Volume % Carbon Dioxide I'ercent 1.90 3.20 0 , Volume % Oxygen Percent 18.70 15.00 N,&CO Volume % Nitrogen and Carbon Monoxide Percent 79.40 81.80 Vms1d Volume Gas Sampled (Standard) d"r 281.036 275.981 Vw Volume Water Vapor "r 48.187 47.678 BWs(measured) Fraction HlO in Stack Gas (Measurcd) Fraction 0.146 0.147 Bw s (saturated) Fraction HlO in Stack Gas (Saturated) Fraction 0.142 0.155 Bw, Fraction lhO in Stack Gas * Fraction 0.142 0.147 Xd Fraction of Dry Gas Fraction 0.858 0.853 Md Molecular WI. Dry Gas Ibllbmol 29.05 29.11 M, Molecular WI. Stack Gas Ibllbmol 27.49 27.48 %1 Percent Isokinetie Percent 102.2 102.6 AVG T, Avg Stack Temperature 'F 120.3 123.7 122.0 A, Stack Cross Sectional Area Sq. Ft. 1.767 1.767 PG Stack Static Pressure In. H20 -0.080 -0.080 Pb, Sample Port Barometric Pressure In. Ug. Abs 24.53 24.58 P, Stack Pressure In. Ug. Abs 24.524 24.574 Q, Slack Gas Volumetric Flow Rate (Std) dscfin 1.28E+03 1.25E+03 1.26E+03 Q. Stack Gas Volumetric Flow Rate (Actual) cflll 1.99E+03 1.97E+03 1.98E+03 V, Velocity of Stack Gas fpm 1.13E+03 1.12E+03 1.I2E+03 Curies Radionuclides per sample pC; 55470.0 70410.0 Crad Concentration of Radionuclides pCi/dscf 197.377 255.126 226.252 ERrad Emission Rate of Radio nuclides pCi/hr l.512E+07 1.912E+07 1.712E+07 * I r the measured moisture content is greater than the saturated moisture level (supersaturated), the saturated moisture va lue will be used in all calculations (40 CFR 60, Method 4, Section 12.1.7). Dryer Baghouse TABLE V COMPLETE RESULTS, PM DENISON MI NES CORPORATION YELLOW CAKE DRYER BAGHOUSE Symbol Descri2tion Dimensions Run #1 Date Date 8/2411 0 Filter # 5606 Begin Time Test Began 9:24 End Time Test Ended 12:19 Pbm Meter Barometric Pressure In, Hg. Abs 24.60 ~H Orifice Pressure Drop In. H20 1.325 Y Meter Calibmtion Y Factor dimensionless 1.010 Vm Volume Gas Sampled .. McterConditions " 87.837 Tm Avg Meter Tempemture 'F 87.8 "~P Sq Root Velocity Head Root In. H2O 0.5138 Wtwe Weight Water Collected Gmms 23.2 T, Dumlion of Test Minutes 120 C, Pitot Tube Coemcient Dimensionless 0.84 Do Nozzle Diameter Inches 0.2745 CO, Volume % Carbon Dioxide Percent 0.00 0, Volume % Ollygen Percent 20.90 N,&CO Volume % Nitrogen and Carbon Monollide Percent 79.10 Vms1d Volume Gas Sampled (Standard) dsef 70.583 Vw Volume Water Vapor $Or 1.094 Bw, Fraction H20 in Stack Gas Frnction 0.015 Xd Frnction of Dry Gas FrnClion 0.985 Md Molecular WI. Dry Gas lbllbmol 28.84 M, Molecular WI. Slack Gas lbllbmol 28.67 %1 Percenllsokinetic Percent 96.3 T, Avg Stack Temperature 'F 113.3 A, Stack Cross Sectional Area Sq. FI. 1.396 PG Stack Static Pressure In.H~ -0.20 Pb, Sample Port Barometric Pressure In. Hg.Abs 24.53 P, Stack Pressure In. Hg. Abs 24.515 Q, Stack Gas Volumetric Flow Rate (Std) dsclin 2.07E+03 Q, Stack Gas Volumetric Flow Rate (Actual) eflll 2.79E+03 V, Velocity of Stack Gas fpm 2.00E+03 Curies Radionuelides per sample pCi 2742.1 Crad Concentration of Radionuclides pCildscf 38.8491 ERrad Emission Rate of Radionuclides pCifhr 4.835E+06 M5 Nomenclature %1 = percent isokinetic, percent A, = stack cross-sectional area (fe) AS~P = see -.j~P Btu = unit heat value (British thermal unit) Bw, = fraction of water in stack gas Cu = concentration of particulate matter, back half (gr/dscf,lb/dscf, etc.) C,= concentration of particulate matter, front half (gr/dscf,lb/dscf, etc.) C""", = concentration of metals (ppm, "glft3, etc.) atomic symbol replaces "metal" CO, = percent carbon dioxide in the stack gas Cp = pitot tube coefficient (0.84) C -species symbol replaces x . x (avg)- Cx (WIT) = actual gas concentration corrected to required percent 0, ~H = orifice pressure drop (inches H,O) L'lH@ = orifice pressure (inches H,o) ~P = stack flow pressure differential (inches H,O) D, = diameter of the stack (feet) D" = nozzle diameter (inches) EA = percent excess air ERB = emission rate of back half particulate (lb/hr) ERr = emission rate of front half particulate (lb/hr) ERmmBtu = emission rate per mmBtu or ton of fuel etc. ERx = emission rate of compound which replaces x k-fact = multiplier of test point L'lP to determine test point ~H L = length of rectangular stack (inches) mBtu = thousand Btu Md = molecular weight of stack gas, dry basis (lb/lb-mol) MF = mass of particulate on filter (mg) Mrp = mass of particulate matter on filter and probe (mg) mmBtu = million Btu Mp = mass of particulate matter in probe (mg) M, = molecular weight of stack gas, wet basis (glgmol) N, = percent nitrogen in the stack gas 0 , = percent oxygen in the stack gas -.j~P = average of the square roots of ~P (may also be referred to as AS~P) Pb", = absolute barometric pressure at the dry gas meter (inches Hg) Pbp = absolute barometric pressure at the sample location (inches Hg) Po = stack static pressure (inches H,O) P, = absolute stack pressure (inches Hg) Pm' = absolute pressure at standard conditions (29.92 inches Hg.) S = time of test (minutes) Q, = stack gas volumetric flow rate (acfm) Q, = stack gas volumetric flow rate (dscfm) Qw = wet stack gas std. volumetric flow (fe/min, wscfm) T, = stack temperature (F) T"d = absolute temperature at standard conditions (528°R) Tt = seeS M5 Nomenclature um ~ mean molecular speed (cm/s) Vm ~ sample volume (ft3) at meter conditions Vm"d ~ volume standard (dsc!), sample volume adjusted to 68°F and 29.92 inches Hg. V, ~ velocity of stack gas (fpm) V wo ~ volume water vapor (sc!) at 68°F and 29.92 inches Hg. W ~ Width of rectangular stack (inches) Wtwo ~ weight of the condensed water collected (grams) Xd ~ fraction of dry gas Y ~ meter calibration Y-factor (dimensionless) Method 5 %1 = Ym"d ' (T, + 460)' 1039 / (9· Y,' P,' Xd ' 0 "') A, = (Os' /4) • 11 Bw, = Y w / (Ym"d +Y w) CB = MB ' 0.01543 / Ym"d Cr= Mrp' 0.01543 /Ym"d Cx (,orr) = Cx ("g) • (20.9 -desi red %0,) / (20.9 -actual %0,) D,q = 2 • L • W / (L + W) 0" d" = "{0.0269 • (Pb", + 0.0735) / [(T", + 460) • Cp • Xd • "[(T, + 460) • M,) / (P, • 6P)]} EA = (%0, -0.5 %CO) / [0.264 %N, -(%0, -0.5 %CO)] ERa = Ca • Q, • 0.00857 ERr = Cr' Q, • 0.00857 ER",,,,u," = ERx / (mmBtu / hr) K-fact = 846.72 • On 4 • 6 H@ • C.' • X/ • Md • P, • (T", + 460) / [M, • (T, + 460) • (Pb", + 6H / 13.6)] Md = CO, • 0.44 + 0 , • 0.32 + N, '0.28 M, = (Md ' Xd) + (18' Bw,) P, = Pbp + (Pa /13.6) Qa=Vs·As Q, = Qa· Xd • Ps' T"d / [(Ts + 460) • P"d] Qw = Q, / Xd Ym"d = Ym' Y· T"d ' (Pb", + 6 H /13.6) / [P"d' (T", + 460)] Y, = 85.49' 60' Cp' "61' • "[(T, + 460) / (I', • M,)] Yw,= Wtw,' 0.04715 Xd =I-Bw, APPENDIXB North Yellow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data Yellow Cake Dryer Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data B North Yellow Cake Dryer Scrubber Pn.~lim 8 pts blank Facil ity Denison Mines Stack Identification North Yellow Cake Scru hher Date tif !7.<1!oV i llal'OT11Clril' Pressure Ph", :v+~ 6 in Hg Pb,• l-'1.53 in Hg N '0 Static Pressure (P,,)-O .D'I in 1110 Estimated Moisture (l3 ws)_~ % Sample Height from Ground __ 1:2-fl:cl A COIl11Il ClltS: Stack Dill 18 Rctcrcilce 0 l'orts me 9.5' Upstream from ncxt <hstllrb.'lIlCe Porls arc 9.5' Dmvnslr\'<l11l from 101,,1 disturhallcc Traverse Percellt Distance From: Ports I'oillt Diameter ID ncfcrcllcc A B C I) E F - I 3.2 0.58 0.58 '·'>'''.3 ft..~~ .. 2 10.5 1.89 1.89 ',.., o}} '~:j.,!> 3 19.4 3.49 3.49 ,z.( .oH' 'zo-,0 n, .... 4 32,3 5.81 5.81 t ~.r ,of'( '~'H' I V7 ·tJ~J,. ~. 5 67.7 12.19 12.19 ,0 ~I 0 6 80.6 14.5 1 14.5 1 1..-. of f.... I."~ ... ~- 7 89.5 16.11 16.1 1 I ~ . o 'IS:) ':"'0"1 0 8 96.8 17.42 17.42 ,u 'off ',v'/) ~ 0 Averages: L Flow --- -iL\\' ---6 1' ___ _ KEY => t ~ Field Oat:! Sheet Plant: Denison Mines 0", 4\ 1.."\\ It> \ ' Tr3'C'~~ Tunc I DGM I 6 P 6H ("1'1;0, Porn. Clock Min CO) (B', , ... u,o. DesIred Actual Fill" 5~. \ TETCO 11 ~ Sample Box 1+ yv~ Location: NortU:0wcakc Dryer Scruhber Opo:r,ltor: __ ~~I--' DGM Temp cr.,) V,,""m 1---r--'-"'i=='T'- , ... !IF) St:lck cr,) FIlter Emu!:"! II QuI I In Page -L-or z.... Run 1#_1_ sO t N A :=q (/·\5 0 q'l.-t','J.v5 ,o<.t, /,/2-J./ L-'/..-Wt 1.:, r z,(.O 'u'n ' (P r -.f-r # I ') I ',),~~·o'i ') ,~"'; f.1 ~ (.1 1.-'V itt 1t:!/Z&'l--t-~ {p~ $('1-'b'L 5",'0"m""_"'_ Pon Rcfcrcnre _0.0·_ 2 :'0 <j<{C(. );,z, '000 1·0-1' /.-1-'1/ liP[ t-Ip() 1-c,> '2-ro &c;-Vt-'1-+ Pon,,,, 9.5' Up",,,m fco",",,,dlS!ulb,,,, 2 '-is '15''6.,,'6 '0(,1-/·/u 1'/0 -" 12-1 '2"{) 2-~;, 2-,-q-:;;, '1 \ IO'!.-Poll,,,, 9.5' Dow''''"m floml",d",,,b,,,, 3 !J 0 "'l ln<,{ t; z!1 'Ol.-S" 1,\ '" H i1 -"0 I-z.-o t:,'-I -z.---l '{ -z,-I-z.. ~'-"f~1 I c>L-Ass.m,d Moist." 4,13 % I'''-~ 'l-, "1-"1.101 '6(,~ (·L'7' \.\'5 -" /1'1> I w,~$.'-,-,<..f 'Z'1 I t-,--1! Cf{; )01> plob, -zrG Cp ~ ':1" 4 <]0 %-q'SI-, ·ors 1,'11-IL,"! ~ IVC> , 1jc{,'< 'i<.j., l.?j qy l it> ) .. -<, 4 l OS IOOG-,:rz--) o~V/-s-1 I,) .; I~'i -Z,:;OZY.'S' Z'lc u'; ,"1 /l:? 1-00 5 11.0 IOiZ:iO D 'O~Dl':1r l.1 Ir -z,lt t~'i1_?f 'l.--7'l,.-:(g~ 11"1 1£'1 In< /0'lf1, '].Ut--'D'il; J'1' I,,. (p 1/'l-!P U ~30'1.-7\ t; f-leb fJ~ Noule Calibration ,3.J:..! ,;>" 1 .>,,"" ,3~"" A\-g On . 3¥ I t Ginchcs G"1J'S~07 " i· ~ "> u· ., '0 -<&'" ~oc 5 .Lj!tl:Oll !<cD lo3(P ,t;~ol 'OGtY' f "f . 1,1-'<, +-{'L 't 1-'-'\ -z.~\ -z.':"(..-{g /00 1\ JUI T; I ~S' I05'().OC..f I ·O~C 1''1~ {,villi -i.lt."\ t'" .1;~\O'Z-;\ (;, IQl II -;-6 7 I '/«0 IO~I .<'/'i'1-,f:/W7,iT~ {"f'!.. 71 1"15> (o'H,W\ Ot~ ,·'\1--I,Y1 81 2-/0 10'6;'.<64'101-5 n r \'') r 6 'Vz,.<) II I [)'1),}"511~ 1;,11 (~'[IF3'7.r<' II--(t;t-l 't{j >It'1 \ 1 <.{ '<51 (;-+-11 {\/ \ I II i /z;t'6j 1--1vII IIO(P , :;0>' ~ i j l I i I I. ' II ' ~H FI B ,I'li 1\ I"olll { 1-<f,G'i 3 ~....,..,....~-=-O/ M~ ~ I H ,G~"\ --- y. 1 A --~-* , .. ConSOlC_~_--,-_ Y-Factor J. 0 0 0 ~H~ ~"",",o lJarOIIlClfh: Pf\:ssures I'b. _~..':i±~ '" II. 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(.7) 5 1,-0 -z.~6 27"-ZTO (,,2. 103 J1 ;7. 1-0> 7 '<U ~O.()~", -JL'6i> /.'-{{. 1·% IP. /1,,0 rJ,<-(1..-l.(;\> ~~<;" 5<)' /0) 111- ,,-7 '13$' z,lPl. ,z.y .,,1-5 /·"'-d t·'!" U' I 'l..V ~5 \ 1..-iJ1 'l.-lu5 5'1 I/O? wt ;0 8 'i>-" ZTL..·\c;-s:: .~1-'-5" .,,}-.1-jY (t71\0t. ~C(i -z..'\ 'l,.1oG>li"D JOe{ 1/+ .... 8 <.{~ t.¥)I)';'V .(>t~ I·"'ll' (.--l i.. +-ltV -~n 1-191' 1.&-11 &'S to: Ills ~ o~ Ij,,:<{r, '-ii''' 2.'1":>.'11'-1 ' ~ "'O~.J"\ J 1 ' S ~<· I II /1.i-.',,~ 1 ~(p ,1."1.'- Pagc~of L Run #~ i N BO A Slack Diameter 1 8~__ Port RdCrcn;,.-c _ O.O~_ Pons ;lfe 9.5' Upstrc:lI11 from next disturbance POrlS arc 9.5' DownSlrcam from last disturbance t\ssum..:u MoiSlun.: 4·13 %. Pro!>:: t. t \0 CP~ Nozzlr.: Calihration ~~.~ :¥10 Avg On -;'8"1 ~C; inches G3sBJg \-1 ~O r Console -:,- Y-Fach.lT l.o.>o-'" m., l·"" )'1 '" 1(,0 Bawm::lric !'rc~ur~'$ Ph",_.t.t.{· _~In Ilg I'h,. __ ..1-~ ;, _;" ," p(;._ --:...Q .O'r __ inll,O Lc~1. n' .... ~1. I'r<.: :1'/1',,,6 .01 --z,.. 'J" '" !!,~ 1.. Y I'UQII\~I~ o· 0 Iotll:O 0.02; 1\')01 O-:Oo ~ 1'1- 0.0 (). 025- '1:>[."\' ') \ \... ,"'\ . 0'7t.7 ..... ...\ 11 ·51:> ,-~~t7 l ·'-{5~ 7;>'6 50 ['/..0 .7 {g r:' \L-- I OS'V W:ncr Coll:;ctl:d (0 -z...--z.... ,.. -rt ' line S;lIllplcd . 0 nlln RC\IC\\ 1,)1:11 Ku :lll,,, ,\vcr:lgc I~ '" flU ", Additional (Ex.tra) Leak Check Information ,,~'¢* } ,,'S Rate (felmjn) IV'. ,,~ Rate (fe/min) OGM before leak Check Vac ("Hg) (J OGM After leak Check Vac ("Hg) { q '6'.L{ ( /p I -:t-0 '00 '0 In,rYL / i'6'''1''\()O '2-\ O·OU,,\ I { I 1'd j ~ Field Oatl Sheet _ TETeO I}-Filter~ 1-Slmplc Box ___ _ ---- '" z. .. , " !F" t-. 3 ,~'- h- >' " ,-7110 Plant: Denison Mines 1 O"e-({1'U~ 10 ~_s: Cat~n~North cllowcakc Dryer Scrubber Operator: ---4--'''-+ Tro.,~r:;c Tun.: DGM ~p ~H 1 .... ,0) V:acuum TempcratureS,Tt 1>Gt.l Tcmp(T,.,) PO"'I Clock Min (0) (/to,! ( .. 1100, Desired AClual \""" S13Ck (T.) Probe Prulx:Ou! Filter Emuent Oul In 1 y!;"1" 0 1.'1'-1-1'0'Z _()O-z. /-JO (-10 -~ /'IP 1.51' 1.-310 &,>, ~& IS 'l-'-f 1 1'7 ~D'1_).-+~ ,0&1.-I'/() 1-10 ''71 11..-1 ZLfv Z;j-< 2-<-'-{ te:5 KJ 15> 2 ,0 \I\,l(>U ,0(,,:' I.I~ /1"-~ 11--<---?-II// 0\0 ~S-/;,<;;--3) '1~ 2 4<; >'2,-1-;1'--ottD /-01 j-O '7 I'Z-? -ZS'1l-&1 '2-" 14 'if1-'1<;{ 3 (PO 7,-,>;,_'1C>!) 'Di;O {'o-t -u tt 12 . .2, 7..1.'" 1..("tl '2.(" i.R&! ~"J 101 3 1-<; ,,>'f)·'V) ·",,2 /·Il-.It--'-j 11"\ 2<-(" Z0"It..~i-5'1-'1.( /0,:/ 4 10 ),-).2-\ -ob I ·~..j . .>-'1 <J IV:; Z-'Z,"1 1.5> 1-q!7 5 G "1;' tD':> 4 10" )~'1 1-z,'1o"l'" /.'}1.-,·n V 1'1--" 1.-'10 V::, '1-s-l 1.-0 'I;' tD -}- 5 ho J ·{f·?H, 6,,](; HrJ I'r"" 1:' 11--'1 1-~y -z5Zj'1,--~ (,,7.-45. 10'1 "'" 5 i}<;' g'1./0-70'i~ I·'H-VH '?' 11.'; '7-1.:. "1.-5'11 V,') &-7 j-j li- 6 lSI> t.{O/.S-r.[) '0'\5' 1·11-I·r-z.-II> IVt 'Z.:P z.~'i 1'1_;1 i.R 48" II t:. 6 I,n ,,," I~" l.{1'S ,;}-b'{ ·O~ ('f} !·t1-/1, 17K-2-7 z.Y [1_,0 IP q~ II", 7 ":0. I~O U.U·Z-bO -0&'/ {-1-C { (-"-'1 /l..c, z.S1l 7-«V l-'-("i >1-'ir t! -j 7 I ~" 1-11,-:}-\((;'l.. -DK 1-1-1 {·"Or ? pv l.r.{~I ?'·{S I t.<{:}-~c "15' fa, 8 z,IO <-/'-1'6'./"1'3 'bt-£ /-ti" 1·'Z,'r~. I?-'(( 7.-'7--& 253 2g~ ",-1' "11-lo@; 8 ttS" t-{c;B"·h1 'Cl(.C, l -t'1 II·V 1 '1 "'D 1..-S-~ 2-5) 2-« >v "lit 10"'- n'O~ 'Z,'-!0 4~q .(qf, f]y.·I ,Y , -/.I$'1- / r::, 3) _ _ l n 1 Tot:!1 -------,--- A\'cr .. g~· , Fil • •• __ • r •••• ,... ••• ::;0-., _. E;c.tra Leak Check Inf' ~ .. »-.. -.. O'~ 1'3£cLof ~RUnp.-3=- i 80 N A S13Ck Olamcter I S" __ PorI Retim::ncc _00"_ Ports arc 9.5' Upstream from nC.~1 disturbance Ports ~rc 9.5' DOWIlStrC3111 frolll lasl disturbance Assumed Moisture 4-13 ~o Probe Z i-G CP~ Noulc C3hbr:!.lwn .:3 .n-.:....2li -3.r~ . 3J' 0 A\'g Do . ~E-/ ZSiiich~'s G35 U3!; tfc. -$ J Console r Y-F:Il;t\tr ! ~ r.> 0 0 ,\H., 1 _ Ss.l'< 11,0 ]J:Jrom.;uic Pressures Pb '2 '-t. ,~-milS Pb'·' ·i.-V"S-~ . 11111;,: " ---:-~-::-~-~ Fe;. ~ <:). Os;.--IIl11z0 L~a~ ('h,'~;" I'IC ~ I":.';""n CJ· 0 ] 2- 'l~ n: ll~ z."2. I'nol Ka;~ ~, 11,0 ~S' 0.0 W3ter Coil::cl<.:d g Tmw S;ullpkJ ~ Er 0 mil: J{C\I;;\\ lEi K -i!:T~, K"" 1I'T", ~ C~r.tW Rate (fe/min) ~ostDGM P Vac ("Hg) 1 Rate (ft3/min) Pre DGM Vac I"H9) '-(-z..~.o4) i ~ 0001-'fL(P ~z,'l;o/ '1.1.-1 0 . OIV I ~.ln-) ~ Field D;;Ha Sheet Plant: Denison Mjm::s , Dat" 5i--L/-"Z-'S:::cJ-"z.~. I .... > ____ _ r THeo /1 filler >b 0 t Sampil: Oox._.:.'=-:J _ 'i&6l' S'L. 0,,\ --- Location: No Yel lowcake Drv\.:r Scrubber Operator: k -f""--f T,~,'c'sc Time lXir-.'1 I.1P I 6H (;"H,Oi \'3cuum Temper-rImes ,"J, DG/>.I Temp cr.J Po,n, Clock Min (0) i.1', ~ Dcsir~d AC\u:l1 , ... ". Stad; cr,) ProOc Probc:OuI Filler EfTIucnt OUI In 'i o· 1 IZ:D'J z'/o '1t.'j./,1. -~'6? 1·5'( l"S'I <-; 11. i-'u5Y Z-S"O Z.'{':1 _"'1. '12'. IOJ.e. ", 2.S, "!,{O'1 ~'( ."~'i /'55 /'J-~ <-) 1'2-"0 2'1 1..<;1.. 2", ->'1 "7& l o r P::Igc f:-_of~ Run /j z i BQ N A Stack IJI:lmCICr lK~ __ Pon Reference 0.0"_ ,... 2 2.}0 'f "i t ·.o 3~ . (?!rS [. Sy-(. 'f'c.; U J7.. 'i( V-r) v,,, 't-5<j 5:1--"1-+-I i h I'on, "" 9.5' Up"'''''' 'CU," n,." d'"",b,,,,, ~!> 2 Z3-S-SO·".JO'L--vI{:' 1'51 I.J'" I I; 170 v7'i lc,---;, t~-z, ""'1 "1'1 /1-1..-I'on"" 9.5' Do",,,,,,,,,,,fw,,,I,,,",,,,,b,,,, :> 00 3 360 <:;"(('.~~? 'b'ttp (.t;<!-I·.~: '..}-//-2.-"iZ7.S'Z,V;t. p) JOt W-/ A""""d Mo',,",, 4-1 3 " ., 3 315 1 c;,-~-r'HJo'lo /.(p'-1 .(pl c;< I ~-?AV1_~ z,,¥' ,"}-l e \ 11r.... Pcob, '2.1-&--,0 4 3:51.i ln "i.I1-S--O~( I·('v{ 'Il \ Ie;( rL:1 1-7 7.:; i..~<)tJ(O IDt.-/I t ~ 4 "S'iS 14"51 .7X'> '0';'5> 1 5"'-\'S''1 q (7,.1P 11,"'~ '2-5 7,e:t: •. -{o-" tn' (p ,..,. 5 3 b () I <;"(p Z. . tH"Z 0 'i s-/. '/-'t. . HI) 1\ '7 1--'": 1/~ • 1--C:J :0 ':> I oS Wi -Ir .,-5 :','1-$ 51-(p.6'<o~5 (.§~ I,,~I < lh IU 1?Sc{ '7flZ,~,? "'j(P ID! ;~j >'" 6 3'l<.l i 5~rt-5l.u ·o~o ("H \.-{I.? /1.,0 '1-5 P 11-:> ~ ""_'V '1 t lOT ~, 'is 6 <f~r ,c;'16 .(,'-/, ,Ott (.1,C( (.1..'6 ", /1,.1.-1--<;-\ '1 . .<':;'0 ~S--t ~+ '1"'l ,iI 1--0<> 7 "~<.l (goC1-2.~ I -o(,§ \.1"1 1·\ -I. L Il~ -t"'/I t---<'o vi (; /.D JI-z... .. 7 ~3o l,t'1 ·"IH .D/'~ {.1,'i I·'vi /.. 1'1-0 1.'-\ 1..'\1-ZI-{ 5+ (01 1[3 ;-a 8 I'iS'':> w1..Q .Ql'i -01"V I V< 1'1.'( 7 11-.0 Lot,\ Z;-t5 Z"\"1 "l 10 Ii<-{ ~=:iJ *,' (,'lu·tz.-z... -OH (-1."/ '1--, VJ IW 'lAo) -v-,'1> Uio 0f f oz.. !Ii ~ ." ---J I ~.~", <..f &-v (,$' L )'II.-' • • I I~z..-·I'i" -<iOOJ 1'61 · Y'/1' i' '* I II') 1]>.3-YH- ---11~llllil' j~Hr--t-iH , rOl:l1 ,\ .. n"",!;" "':,&''1. \.1\ _~"':":""~_-I ~.qtl,v .'!-t~ , Additional (Extra) L~ak Check Information c..tS"') I .-{(t- ? ;'6''6" \ -z.,;,.1- k~~ )<1',1 \, (,'Sl ' '" ,?~~T Il."~ DGM befO~ Leak Check Vac t"Hg) I Rate (ft'/min) . b6'GM After Leak Check :;\J:~ 0r) 1 \ :5'&1. vt> \ L ,,"'''''''\-_\W> 4\~v ')* . 1-\ I O.{)! 0 I . " -., \v\~.~~ S".i-.~z.,\ ~<R~.OIO 9 .... " , ,.-v _ L tI f \--\ GL{~V I {)('--( Vac ("Hg) 2\ CP ~ Nozzle Calibration .-Wl-.'S~I .:,y"!.-.3~D A\,g Dr.~~~ Go> Ihg i-\ [, -;. Console ---=x. Y·F:.tctor /.000 l.\H;;J~l H~O Uanlillctric Pn:ssurcs Pbr.. _ '? '-{. (, ,. In !lg Pb,,_.k.~$ __ mHg 1\ -(). 6 ~_In!!:;O LcJ\,Oed !J];: !Jill 0'0"5 II',,,,,,, 0,0/"(.... ''Aml l!: 1'"", R:ue bll:O 'l.'t-- o . ~Z S- (J-e> 13 C·M.) O·() (GI)."2.- \\';)Io:r C\l]kcICd g r."" ,""""," ~ 6 "H" l{o,:\lo.:W K= @l':I .. (i,-" -.,,' Rate (fe/min) o·()()'6' Yellow Cake Dryer Baghouse Prelilll 6 pIS blank Filcility Denisoll Mines Stack Iden tification North Yellow Clke Dryer B<lghollsc Date r Baromctrir Pressure B Pb. in Hg Phi' in Hg N 0 Slatic Pressure (PrJ in \-110 A Estinl<ltcd Moisture (Bws) I %, Sample Height from Ground feet Comments; St:wk DI3 16 Refcfenl'C 0 I'mt5 :vt': 57" Upstretlill frOIllIl(').;\ {hSlmhancc I'orls arc 46R" Downstream from last dlsltlrlh11lcc Traverse Percent Distance FI'OIII: Ports Point Dhlmeter 1\) Reference A 11 C D E r I 4.4 0.70 0.70 2 14.6 2.34 2.34 3 29.6 4.74 4.74 4 70.4 11.26 11.26 5 85.4 13.66 13.66 6 95.6 15.30 15.30 t\ vcragcs: Ts __ _ L Flow --- ill' ~6P ------ KEY ~> 6 1' -I ~ § " ~I ~I V) , .-z ~ 0 .= --~:r' § ("J !C:_ • o 0 0 0 '" ~ § i:-~ , ~ ~ ,~) ., 0 t" N r-I North Yellow Cake Scrubber Sample Recovery Gas Analysis Data (ORSA T) Yellow Cake Dryer Baghouse Sample Recovery Gas Analysis Data (Ambient) Chain of Custody Lab Analysis APPENDIXC c North Yellow Cake Dryer Scrubber Method 5 G imp Facility: Denison Mine Dmc: Slack Idenlification: c..N:..:Y-,C",: S"'c::.n::.:lb"'b"'el:...· ____________ _ --- - -. IMPINGERS Filler Num ber IMplNGERS riller Numbt!r 5~i)1 IMJ'INGERS Filter Number lMPINGEBS Fi Iter Number Final (~) Inilial (g) Net (g) Run: drop out Run: drop out , ~l o8 ·D ..,1. r· l' ~tl.o_ :3 Run: drop our J Sample Box: I-} Impmgcr Number 2 :I I 4 I 5 Inillal Voluille of liquit! (H20 ) in imping('r!>, (ml) I 100 I 100 I Silica GeT] TOlal (g)=",;I,,;O~2~-Z=.,,!,lJb= Sample Box: Impinge .. Number 2 :I . I 4 I 5 Initial Volume of liquid (HP ) itl impillgcr~, (rn!) -I 100 I 100 I Silic-I Cel . , , ~~ L t:. C()'z... Ip Lq'/(,. :> 1.1f).r'{ 1SZ.,(' .n'S·", 1·/'1'7 (,/5 t (0).1 '6 "1 y-. -V lS'1 ·-1 2.l ~ . ( 3~-f., 15'.IL. ,)'-( ,3 TOlal (g) 10 It. z.. Sample Box: Impmgel' Numbc,' 2 3 I 4 I 5 6 Initial Vl)IUIllC (lfli(lllld II ii » 111 illlillngcrs. (1111) I 100 I 100 I Sil ica Gel Fina l (g) ___ -+ ___ --+ ___ -+-___ + ___ + __ Initial (g) ___ -+ ___ --+ ___ -+-___ + ___ + __ _ Net (g)===d,===",====b==d,===",=== TOlal (g) ====== Run : Sample Box: Imllmger Numbcr :I I 4 I 5 6 IlIil1<11 Volume of liquid (Hi)) ill illlpil1g{~rs, (ml) dropout I 100 I 100 I Final (g) ___ -I ___ -+ ___ -+-___ + ___ + __ _ Inili.1 (g) ____ I ___ -+ ___ -+-___ -+-___ + __ _ Net(g)===~==="'====l===~==="'==== TOlal (g) ===== Plant Location, __________ _ -----------A nalYI ical Method . __ JOlJR'iS;,· A!:UT __ _ Date 9/-t<1 Ill) Tcst No. -....,.;/~......,t Gas Bag No. H -~3 Ambient TemJl_!t-P~. -"",5:.......- Operator_~~z.:~::...! ':"""'_ Date If /z. $-/, 0 Test No. _~1.--::,...~~ Gas Bag No. _!JH'c..;Ce..-"...::."5_ Ambient Temp_--JU'"",b __ Operator_....If±1:..:::l._ Datc ____ _ Test No. ____ _ Gas Bag No. ____ _ Ambient Temp ____ _ Operator ____ _ Gas CO, O 2 (Net is Actu:l1 O2 Reading Minus Actual co, Reading). N! (Net is 100 Minus Actual O2 Reading). GlI.Ii CO, O2 (Net is Actual O2 Reading Minus Actual C01 Reading). N2 (Nct is 100 Minus Actual O2 Reading). Gas CO, O 2 (Net is Actual O2 Reading Minu s Actual CO2 Reading). N2 (Net is 100 Minns Actual O:! Reading). Aftml! R,~ading 1-/ -ZO·" (':H.'c', , ,,;-. :>-,l; ::~~ to{' -' -/.~~ Attna) Rl·;uling, :,,1- I &-c E- ' >!:? '/"'t Arlual Ilt·;Hlin~ 17 .~ '·,-1. ; -; II UN I 2 Net Actual n~i1ding /.<>r ! "' I '? .1-Zu· " '\i{ ./. '~ I · " .. it: IIUN I 2 .\et Ac tuill Ue:uling ,,2-).2- I )--:'0 /y.t- , , '. ' .. ~";.>" Il UN 1 2 :\:cl AClual r{cadin~ . .; ,. . "i :o.rl.;:~ .. CO 1$ !lot l\ll"aSIlf~J, (IS 1\ lI:"!s the SiltllC molecular weight as N~ 3 Avcr:lge :\cl Actual Nel Net IlradillJ! Volume /. i /. '7 /'7 1-7 ( 8-. 1 20,t, I !5-':j I tf. :; --,~it-:; ~p ~}ft' I :!~ ,;-.;,\ ' f~:~ ~~,:St:(' 3 Average Net AClu:l! !"1ft Net Re:ulin!; Volume ~. t.. 3·z->. ~l,. 3·1:: I '): 0 I~'~ IS--. '-<,-.0 'fj'~!' II';;~; of t ; .:.<"'&- 3 Average ;\:('1 ;\tlll;11 N("I Net Heading Volume ;'''};:l~ii;i;' II , r-lr!f(,,), Yellow Cake Dryer Baghouse Method 5 Facility: Denison Mi ne Date: _-;;r!f;.<....<)-=-<..'f_-.!-(..::.U_ Stack Identification: .;..N;..;Y'-'C'-Il::.a"'g"'h"'OI;;.:iS:.:.e ____________ _ IMPINGERS Filter Number IMPINGFHS Filter Number IMPINGERS Filter Number Final (g) Initial (g) Net (sl Run: 100 , 105', \ l-l l.S- -(7-.'1) Run: 100 Sample Box: p Impingcr Nnmber 2 3 I 4 I 5 Ini(ial Voluille ofliquid (II~O) in impingcrs. (ml) 100 I I Sihc',Gd I J , , , i.J 11'1·0 S-i (). ) 'ISU' '1 (0'10'1 s-~S·r '1:> Z·" :jl]l S? I '-('S" 11{-·() Toral (g) ====== Sample Box: Implllgcr Nnmbc," 2 3 . I 4 I 5 6 Inilial VnllUn~ of liquid (1 110) in Illlpingcrs. (ml) J Fill.1 (g)------jf----I----+----+---+---- IllitillJ (g) ------~-----+----~r-----+_----_r------ Net tg)====,!::.===,===d,====,=====,===== Tota l tg)======== Run: SfHllple Box: Implngcr Numbcr 2 3 I 4 I 111l1i:11 VOIIIIII~ ofliquid (H20) in iIllJlingcrs.(II1I) Final (g) ___ -I ___ -+ ___ -+ ___ + ___ + __ _ Initial (:;)----1----+----+---+---+--- Net (g) ===d==~==~==~==d== Toml (g) ===== I M PINCERS Run: Sample Box: Fi\{er Number Implllgc," Number 2 3 I 4 I 5 6 Inill;.1 Vulullle of liquid (1-1:0 ) ill impingcrs, (ml) 100 100 I I SHica Gel I J Final tg) ___ -ji-__ -I ___ -+ ___ -+-___ + ___ _ Initial (g) ___ -j~---I----+----+----+--- Net (g)====,====,===d,===d:===±==== Total tg) ===== Chain of Custody Record 'AL· 41""\l\1\U: C/:6nl Tetco -.. ~.------... ~ . Address 391 East 620 South Temperature on Re::eipt __ _ TestAmerica Drin!<ing Water? Yss 0 No 0 THE LEADER IN ENVIRONMENTAL TESTING Proit;ct M8IIaroBf O.!:8 Dean Kitchen 8126/2010 i'Qi6f'/1Cf19~' iAfc.2 Cf):Ic}.'F:zJ( Mmt:cr L4bNumbcr 801-492-9106 -----SitecOOia~ Cily 1~~8 1Z;:~~3 La~Cor.E<t',;f Malysis (Attach list if American Fork ScOff Chrin~n .. n,lI;y.n '~mu mora spaca Is noMed) f ProieCf "".!me N1d l..J;x;duon ISt3tcl CW/icr,l Vaybi'!J NumlJer : Den ison M ine 2010 3rd Quarter <':antr.:l-::tlPufch3!1a OtrJerlQuolc No. I Contain!!rs & MOlfix S I ! Preservstives 0 ~ I -------------~ ::l N ., .. ~ Sample 1.0. No. and DeSCJfpUon i I • " ~ n~1 ~. ± 0 Da!e TIme ~ ~I J ~ \j " ~ ~ ~ (C()lI:ainer.; for 9i1Ch s~mp:q mOly b3 com/)Nd en Cfloline) i " < , ". I C"-I , Rl Oaghouse filter (56C6) and beaker 8/24/2010 t 10:00 X I X , , -.•.. -. -- Rl NYC filters ,5S01,5602,S6n) and beaker 8/24/2010 I 8·00 X i ! X I ! . I R2 NYC filters (S607,S60S,S509) and beaker 18/25/2010 17,50 X ! ; X I , I ! , I I I , , , 0· ••• __ ---- ! I ! I --..... -. , , j ; _. .. '. j ; I ; __ J __ ._ I i : 1 , i i i I I ! ! ! i I I ! i •..• -.... ~_ .. __ .o_O" .. , ___ I --h-I I I _. I 1 i . -- C!Jdil1 01 Cus!tJdv Numbe: Page L o,L I I Special /nstrJctJonS/ Conditions of Rece;pt I Possible HeZQld Id~lilc;Jtion ! ~ amp~ urs;>::!uU ~ Disposa/By UD fA fee "'.3y be 8SSe3$ed if 3!JJ"I7Pfes ele re:~ined o ,Von-H11Zaro o F/:Jmmab.'e o Skin /tfit!ult o Poisx. 5 o UnKn:Jlt'ffl 0 Relum To cr~n! o A,,;hive For ___ Ma;7lh.~ tor.gDf th~n 1 momh] TlJrn Arol.!nd TImO! Raqu1red DC: Rcqlllrcr.JYlf.$ (Spfd.fy) o 24 HoUfS o 4S HOUf2::;, 0 T Cays o 11 Days 02103}'1J C otrwr as cer method ~. Reiit,q",sJH:!d By rfL" }£ ll!~~ .71me 1. Rscelvod 5y ,catc I T~. _1~ _ltt,~L/«..QO 2. ReJ;nqu~ed By -----I"'''' I"me 2. R~,.,edOy ! 03.(6 I (tmo ,,? Rhfon",,;'-./':/Orl J:/" _. . .. _.-n..." T' __ IQV, 'r I~--I Ti,71C--1 ~·RfY".eivt:!dBy Cc:nm;m:s __ ~~~~~!et.:. Email to:DeanorPaul.tetco@tetco-ut.com DfSTRIBUTlON: WHITE -Relufflcd to crie,,' .... "n RZPOfI; CA,'\!ARY -Sniys with /!'.~ $:irr.pl~; FINK· P.eI:J Copy SIlG No. Ol'dt~r No. 42004 TostAmcrica rptSll.nl.'hTill(' \'.\.7.1 'l'cstAmcrica Laboratories, Inc. Analytical Dall, Package Prepared Fur Denison Mines (USA) Corp. Denison :vIine 20 I 0 31'd Qtl' Radiochemical Ana lysis By TestAmcrica 2800 C.W. W(~y. Rich/am/ Wa, 99354, (509)-375-313/. Assigned Laboratory Code: Data Package CfJlltaill,\' 14 Pages Report No.: 44930 Resnlts in this I'cport I'clate only to the sample(s) analyzed. Clicnt Sa mple ID (List Order) Lot-Sa No. Work Order RCI)Orl Dil l D R1 BAGHOUSE JOH 31 0484·1 L6CR51AA 9L6CR510 FIL TER(5606)&BEAKE R1 NYC JOH310484-2 L6CTN1AA 9L6CTN10 FIL TERS(5601 ,5602,5622& R2 NYC JOH310484-3 L6CVC1AA 9L6CVC10 FIL TERS(5607 ,5608,5609& Batch No. 0245332 0245332 0245332 TestAmeric a THE LEADER IN t;NVtRONME.r!r Al Tt:SIINU Certificate of Analysis October 19,20 I 0 Denison Mine.s (USA) Corp 1050 17th Streot. Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab PrQiect Name Sample Type SDG Numbe r I. Introduction Augus t 31, 20 10 Denison Mine 20 10 ]!d QII" Three (3) Filter Samples 42004 CASE NARRATIVE On August 31. 20 I 0, tlucl,."! tilter samples were received at TestA medea' $. Richland laboratury for radiochemical analysis. Upon receipt , the s(tmples were assigned the Tt!stAmcrica identifi cation nUlllbers as described on the cover page oflhe Allal y lic~l Data Package ri;!.port fOl'I11. The samples were ass igned to Lot Numbers JOH310484. II. Sample Receipt The samples were received in good condition and no anomalies were Ilott!d during check-ill. III. Analytical Results/Methodology The analytical results for this report arc presented by laboratory sampl~ ID. Each sct or dain. illcl \ld~s sample identification inf'ormatioll~ analytical results and the appropri(1tc associated statistical uncertainties. The analysis requ(:sted was: Alpha Spectroscopy Uranium-234, -235, -23S by IIldhod RL-ALP-004 IV. QU:llity Control The analyt ical result for each analysis pcrlorilled includes a minimulll of one lf1boralory control sample (LCS), and one reagent blauk sample analysis. Any exceptions have been noted in the "Colllmen"" section. 'I'CSIAmcrica Laboratories, Inc. 2 Denison Mines (USA) Corp October 19. 20 10 V. COll1nH.~nts Alpha Spectroscopy Uraniulll-234. 235. 238 The achieved MDA of the batch exceeds the detection limit from reduced al iquot si z~s taken due 10 historical process knowledge. The sampl e activit y exceeds the MDA and the CRDL. Dal<l is accepted. Except as noted, the LCS, batch blank and SCllllplc results an:. within acceptance limits. I certify that this Certifi cate of Analysis is ill compliance with the SOW and/or NELAC, both technically and for completeness, for other thallihe conditions detai led above. The Laboratory Manag(!r or a designee, as verified by the following signature has authorized release of the data contnined inlhis hard copy data package. Reviewed and approved: Digitally signed E.,.; ... JI'-'" n",,,~) by Eri ka Jorda n 'J-Date: 2010.10.19 15:36:23 -07'00' Erika Jorcial--'----- Customer Service Manager TcstAlllcrica Laboratori{~s, Inc. Drinking Water Method Cross References DRINKING WATER ASTM METHOD CROSS REFERENCES I Referenced Method lsotope(s) TestAmerica Richland's SOP N EPA 901.1 Cs-134,1-131 RL-GAM-OOI EPA 900.0 Alpha & Bela RL-GPC-OOI EPA 00-02 Gross Alpha (Coprecipilalion) RL-GPC-002 EPA 903.0 Tolal Alpha Radium (Ra-226) RL-RA-002 EPA 903.1 Ra-226 RL-RA-OOI EPA 904.0 Ra-228 RL-RA-OOI EPA 905.0 Sr-89/90 RL-GPC-003 ASTM 05174 Uranium RL-KPA-003 EPA 906.0 Tritium RL-LSC-005 Results in this report relate only to the sample(s) analyzed, Uncertainty Estimation TcstAmcric<l Ridd:::lI1 d has adOrll~d Ihe internationally ~H.:ccph.:d approa~h to estimating ullc(,l'tainlil.!s dcscrib~d in "NIST Technical NOll: 1297, 1994 Edition", The approach. "Lm .... or Propagatiun or Errors". involves the idcnlilicHt ion of all variables in an <llla lylicallllclhou which :Ire uSl'd to daivc II result. These variables are rclnlcd In the nl1alyt icall'(~slllt (R) by some rllilctiollnl relationship, R == constants ,) IlX.y.Z, ... ). The components (X,y.2) ::Ife cvalllalcJ to determine tlll;;r contrihut ion to the l)vl:rall method uncertainty, The individual c()mp0lll.:nt ullccrtaintks (u.) an: then combincd u:;i ng :l slatistical lllmid \11;1\ providcs thl.! most proh~ble ovcrall llllct!rt i'\illly \'aille, All C{lmpOnCllt lIn~:crta;lltics arc categoriz\:d as type 1\, eval uated by statistic:llmcthods, or type B, e\,alllah.:d b) olhel' illeans, Uncertaint ies not illclUllcd in Ihc component:;, such as sample hOlllogcneity, arc combined with the component ullcertaint) as the :;t[uarc rool of the sum~or-lhc-sqlJare5 oflhl.! individllalllllccriaimil's, The unccrtainty associatcd with the derived result is the combined uncertainty (uJ multiplied by the cov{:ragc f:lI.:wr (1.2,01' 3), Whcn three or Illore s<lmpit: rcpl icates an: IIsed to derive the :1I1atylieal result. the type J\ uncertainty is Ihe standard deviation of the mean valuc (SI'! 11), where S is Ihe slandal'd d(:viatioll or Ill{: dcrived rC$lIits, The type 13 lIllccrwinties arc all other I'<Hldolll 01' 1l01l-rHnd\lIll components thaI an: I\ot incillded in the standnrd dcviHlioll, The derivat ion orthc general ~I ,a\\' of' Pl'()pngalion or ErrOl'S" eqllations and spc<:i lic example an: a,~~.ila~~~~ ()~~, r~:qlles~" TestAmorica l'(ltGl'l1cr:11I nfo ,'J,72 TestAmcl'ica Laboratories, Inc. 4 o. AClion Lc\' Balch !lias (:OCNo COllnl Errcw (#s) Total tlncel·t (Us) 11,,_ Combilled Ullcer/(lil1~I" (lis). Co\W<ll,(c F,tClol' CIUlL (RL) I.c l.ot-Sample No MoqMOA I'd mal')' Dclci.~lol' Ih lio 11-234/lJ-238 !lsl/M De' Ihl/I'ol l/rel't RER SDG Sum Rrt Allllia Slier Rst(s) Work Order TestAmorlca The QC pr..:paralion balch lIulnhcr Ihal. rdal~s 1;lhnl'alory samples 10 OC samples Ihal \WI"'! PI\:pw\:d <llld amtiy/cd lngcthn . Dclin..:d hy the equation (Reslil i/Expccted)-\ as dclincd by A:"\SI N 13 .. ,0, ('haill (JfCUSllldy Number assign..:d hy the ('Iienl or TestAllleric;I, Poisson (;Olll itilig statisti cs of the !,!I'OSS Silml)le COllll! and h,.ckgrmltHl. The ulleertaill!), i:o; (11)snlute :u\{1 ill the S'11\.": IIllits as the resulL. For Liquid Sdlllilialiull ('ountill~ (I.SC) the batch blank COlllit is the b:ICkgroullcl, All knO\\1l ullcl!J1ainties as:o;ociated wilh Ihe pro!paflltioll <llld :l1wly:o;is of th..: siIlllple arc PI'llp"{!:lled 10 {!.ivc a lHl:asure of the Ullel:11ninty associated with thl: rl:sult, If,. II/(' c:omhillcd IIl/c{,l'miIllY. The IlIIcertainty is ;lbsnlule ,m\! in lhe same units as Ihl! result. The covcr;lgc Ihetor dcfillC:O; till: width orlhe COlllidcllCC interval, I, 2 or 3 stalld;lf(j dc\'iati~lIls. ConlrOlctual Required Detection Lilllit as delincd illlhc ('Iient's Statement OI"Wnrk or TcstAmcrica ··dc.:l;llIlt·· nominal detcetiolllimii. Olkn rdcrrcd til the reporting k\'cI (RL) Decision I,cvd hased 011 i nstnlllll~nt hnekground or bialik, udjusled hy the Eflieicncy. Chemical Yield, anti Voluille :Issoeialed \\'ith the siltllplc, The Type I error pn1habilily is approximately 5%,. I.e=( I.M5 .. Sqlt(2*(BkgnHK'nl/llkgmdClllivlin)/SC'IIIMin))" «('ollvFetl(EfI~Y ld"!\lm*V()I).$ Ingrl:et), FIll" I .. SC mdlHHis Ihe batch bklllk is uscd as a Ille<lsurc oflhc backgwtlild variahilitr. I.e cannot he cakulatc(1 when the huckgrolilld Wllllt is zero, The number a~sigtlcd by the l.IMS so!iw"rc lu track samples ri:eeived Oil Ihe sa1lle day lor H given client. The sam pic Illlmber is a scqllcn liallltllilber assigned ttll:acll sample ill thc I.o{. I)ctectilll\ I.evel hased {Ill in~lnllnenl bal~kgroulld (If h[;Ulk, adjusted hy thl: Eflicklley, (hcmical Yield, and Volume wilh a Type I nud II error probabilil) of approximately 5%. ~'1D(' "" (4,65 '" Sqrl«l3kgrndC'ntlBk);rTl([CnIMin)fSCntMin) I· 2,7 1/SCnIMin)" (COIIVF(;I/(EfP' Yld " Abn · Vol) $: lugrFio:t), For L..')(' methods the halch hI ant.. is ll:\ed as a measure (l l'thc backgrolilld vuriahi!it}, The inslrulllcnt ide ntifier :ls:O;(I(:iatcd wilh Ihl;: :lnalysi:o; tlfthe :o;allljlJc aliqlltlt. The lJ-234 result di vided by the U-2JS resllit. The U-23'I/{J-23!\ ratio lilrnalllr;)lllr:lI1illlll in 1ST SRM ,1.121C is 1.038. R:ltio uflhc Result tolhe MDt'. !\ valli": gr..:ater than I nla)' imlicate activity above h:u.::kSl'Ollnd at a hi{!.h lIo:\'el of c()nfidclle(~, Callti(}11 :o;holiid he IIsed whcn applyillg this factor ami it should be used in CllIlcct"1 wilh (he lJtL:tlifiers associated wilh lhe resliit. Ratio ol'lhe Result to the Total Ullccrlainty. I fthe ullcertainl), has a l:ovcnlge lilctor 01'2 a \,:tluc gn:atcr thall I may indi{:ate activit y ;llxlVe backgroulld:1I approximately Ihe 95% [evcillfcunlidcllee as.'iltll liug:1 Iw()-:o;itled C(lntiilellt'e interval. Clllllion should he us..:d when 'lpplying this [hctot" and il sh\)Ulu be IIse!1 in (;Ollcert with the quollillers associat ed with the result, San1ple Iden tilil:r IIs(xl hy the re purt syslem, The nllmber is based upon the 1i1'S1 five di{!ib ofthl! \Vorl,; Onlcl' Numher, The equation i{cplicall! Error Ralio "" (S-OYlsqrt(TI'l ls2 + TI'Ucf)j as dclincd by ICYI' B()j\ where S i:-; the orig.inal sample r~sllii. 0 is thl: result orthe dupli Cilt..:. TPUs is Ihe tllla llllll.:ertaill ty orlhl~ original !>ample and Tl'lJd i:o; the tOI;11 ullc":11ui nt)' of the duplic<lte sample. Samplc Ddiv..:ry Group NIIIIlI)l:r ;l.ssiglled h)' thl~ ('Iienl or ns:o;iglll:d by T..::o;t!\llll:ric;llljl(lIl "ullpk r(;l'cipl , The sum of the reported alpha spec result:-; I~lr te:o;ts Ileriv..:1I ['mill the ~:lIlW sample exclud ing duplkale result where thl! results arl: ill thl: same .lIIit s. Th~ LlMS soHw,lrc assign le:o;t spcl:ilie idelltifil~l'. The recovery of th ... · traeet' mldcd 10 the sample su..:h as Pu-242 IIsed 1(1 traCl: a 1'1I-2J1)/40 lIIethod, rj)tGclI('f'nlinro d,72 TcslAmcrica Lnbormorics, Inc. 5 Sample Results Summary TcstAlllerica Ordered by Method. Batch No., Client Sample 10. Report No. : 44930 Client Id Batch Work Order Parameter 0245332 FFSR Rl BAGHOUSE FIL TER(5606)&BEAKE L6CR51AA U-234 U-235 U-238 Rl NYC FILTERS(5601,5602,5622& l 6CTN1AA U-234 U-235 U-238 R2 NYC FILTERS(5607,5608,5609& l 6CVC1AA U-234 U·235 U·238 No. of Results: 9 TestAmerica rptSTLRchSaSum mary2 V5.2.7 A2002 TestAlllcril:a Laborntorics, Inc. Result +. Uncertainty (2s) Qual Units 1.33E-03 +. 2.0E-04 UClfSA 7.21E-05 +-45E-05 UClfSA 1.34E·03 +-2.0E·04 UClfSA 2.55E-02 +-4.0E·03 UClfSA 2.27E-03 +-4.3E-04 UClfSA 2.77E-02 +-4.4E-03 UClfSA 3.37E-02 +-5.3E-03 UClfSA 1.61 E·03 +. 3.2E-04 UClfSA 3.51 E·02 +-5.5E·03 UClfSA Date: 19-0ct-10 SDG No: 42004 Tracer MDe or Yield MOA CROL RER2 91% 3.14E-05 9.00E-15 91% 3.14E-05 900E-15 91°/'1 3.70E-05 900E-15 91% 428E-05 9.00E-15 91%) 2.90E-05 9.00E-15 91% 4.86E-05 9.00E-1 5 85% 3.23E·05 9.00E-15 85% 2.74E-05 9.00E-15 85%) 3.93E-05 900E-15 Report No. : 44930 Batch Work Order Parametor FFSR 0245332 BLANK ac, L6GT01AA U-234 U·235 U-238 0245332 lCS. L6GT01 AC U-234 U-238 No. of Results: 5 QC Results Summary TcstAmcrica Ordered by Method, Batch No, OC Type,. Result +. Uncertainty ( 25) Qual Units 5.89E-08 +-8.0E-08 U UCI/SA o OOE+OO +·4 6E-08 U UCI/SA -4.54E-09 +-4.6E-08 U UCI/SA 1.18E-05 +-2. 1 E-06 UCI/SA 1.23E-05 +-2.1 E-06 UCI/SA TestAmerica HillS -(nrsliltfE~p{'('I('tI)-1 as il<'filU'll by A!\'SI :'<1 13.30. Date: 19-0ct-10 SDG No.: 42004 Tracer l CS Yield Recovery Bias MOqMOA 100% 1.28E-07 100n/ ... 1.09E-07 100% 1 U9E-07 98%, 102%) 00 1 48E-07 98% 101% 00 9.62E-08 rptSTLRchQcSUnl II Qllal -1\11:11),7.('(1 for huluu! dl'h'Cll'llaho\'C limilill~ nill·I'i:l. I.imill'rih'ri;, is i<'s~ than till' 1\llte/lllla. T,)I:II I 'nn'r.,c 'nl)!.. 01' nnt mary V5.2.7 A2002 ld('nli fi,'d bl' ~:tnllna scan softwan'. TcstAmcri cn Laboratories, Inc. 7 FORM I SAMPLE RESULTS Date: 19-0ct-10 Lab Name: TestAmerica Lot-Sample No.: JOH310484-1 SDG: 42004 Report No.: 44930 COC No.: Collection Date: 8/24/201010:00:00 AM Received Date: 8/31/201010:30:00 AM Matrix: AIR FILTER Client Sample 10: R1 BAGHOUSE FILTER(5606)&BEAK Denison Mine 2010 3rd Qtr Ordered by Client Sample 10, Batch No. Parameter Batch: 0245332 U·234 U-235 U-238 No. of Results: 3 Result Count Qual Error ( 2 s) FFSR 1.33E-03 1.9E-04 7.21E-OS 4.4E-OS 1.34E-03 1.9E-04 Comments: Total MOqMDA, Rpt Unit, Yield RstlMDC, Uncert( 2 5) Action Lev Lc CROL(RL) RstlTotUcert Work Order: lSCR51AA Report DB 10: 9L6CR510 2.8E-04 3.14E-05 UCIISA 91 %, (42.3) S.B2E-OS 9.00E-15 (9.5) 4.SE-OS 3.14E-05 UCI/SA 91 % (2.3) S.B2E-OS 9.00E-15 (3.2) 2.BE-04 3.70E-05 UCI/SA 91% (3S.2) 9.S4E-OS 9.00E-15 (9.5) ----.•. -------._-_.----_ .. Ratio U·2341238 = 1.0 Analysis, Prep Date 9/30/10 OB :07 p 9/30/10 OB:07 P 9/30/10 OB:07 p Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample .. ---------- TestAmerica MDCIMDA,Lc . Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. Aliquot Size 0.00104 Sample 0.00104 Sample 0.00104 Sample rptSTlRchSample U Qual· Analyzed for but not detected above limiting criteria. limit criteria is less than the Mdc/Mda. Total Uncert,CROl, or not identified by gamma scan software. V5.2.7 A2002 T~SlAm~ril."u l.o.bor:.ttori~s. 1m:. 8 Primary Detector ALP7 ALP7 ALP7 FORM I SAMPLE RESULTS Date: 19-0cl-10 Lab Name: TestAmerica Lot-Sample No.: JOH310484·2 SDG: 42004 Report No.: 44930 COC No.: Collection Date: 8/24/20108:00:00 AM Received Date: 8131 /201010:30:00 AM Matrix: AIR FILTER Client Sample 10: R1 NYC FILTERS{5601,5602,5622& Denison Mine 2010 3rd Qtr Ordered by Client Sample ID, Batch No. Parameter Batch: 0245332 U-234 U-235 U·23B FFSR Result Count Qual Error ( 2 s) 2.SSE·02 8.0E-04 2.27E-03 2.4E·04 2.77E·02 8.3E-04 Total MDCIMDA, Rpt Unit, Yield RstlMDC, Uncert( 2 5) Action Lev Lc CRDL(RL) RstITotUcert Work Order: L6CTN1AA Report 0810: 9L6CTN10 4.0E·03 4.3E-04 4.4E·03 4.2BE·OS UCI/SA 91% (594.8) 1.30E-OS 9.00E-1S (12.6) 2.98E-05 UCIISA 91 % 6.4SE-06 9.00E-1S 4.86E-OS UCIfSA 91 % 1.S9E-OS 9.00E-1S (76.2) (10.7) (570.3) (12.6) Analysis, Prep Date 9/30110 08:07 p 9130/1008:07 p 9130/1008:07 p Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.00103 Sample 0.00103 Sample 0.00103 Sample Primary Detector ALP8 ALPS ALP8 -------_._------.-----_._--- Ratio U·2341238 = 0.9 No. of Results: 3 Comments: TestArnerica MDC1MDA,lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the MdcfMda, Total Uncert,CRDL, or not identified by gamma scan software. V5.2.7 A2002 restAmeri c~1 Lnb(lr::noril..:s, Inc. 9 FORM II BLANK RESULTS Date: 19-0ct-10 Lab Name: TestAmerica Matrix: A IR Parameter Result Qual Batch: 0245332 FFSR U-234 5.S9E-OB U U-235 O.OOE+OO U U·238 -4.54E'{)9 U Count Total MDClMDA. Error ( 25) Uncert( 25) Lc Work Order: L6GT01AA S.OE.{)S S.OE.{)S 1.2SE·07 3.34E·OS O.OE+OO 4.6E-OS 1.09E·07 2.36E·OS 4.6E-OS 4.6E.{)S 1.09E.{)7 2.36E-OS SOG: 42004 Report No.: 44930 Rpt Unit, RstJMOC, Analysis, Total Sa Aliquot CROL Yield RstiTotUcert Prep Date Size Size Report DB 10: LSGT01A8 UCI/SA 100% 0.46 9/30/10 OS:07 p 1.0 0.27 9.00E·15 (1.5) Sample Sample UCI/SA 100% O. 9/30/10 OS:07 p 1.0 0.27 9.00E-15 O. Sample Sample UCI/SA 100% -0.04 9/30/10 OS:07 p 1.0 0.27 9.00E-15 -0.2 Sample Sample Ratio U·2341238 = -13.0 -------.. -------------_. -_ .. ----------. _ .... _. - No. of Results: TestAmerica rptSTLRchBlank VS,2.7 A2002 3 Comments: MDClMDA,Lc -Detection, Decision l evel based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. l' Qual-AII;ti}J:eJ ror "ut Iwt dt'lcCleU abU'l· iimilin:; (;rilt"ria. Limil crill'ri:l is less Ihan Ihl' ~llkl!\ld:I, Tolal l1nCl'rl.('RDL, or nvl itit'nlirk d b~ ~allllmi lOt'an svrt"lln·. T~Slr\m~rka l.ahor3!ories, In!.:. II Primary Detector ALP10 ALP10 ALP10 Lab Name: TestAmerica Matrix: AIR Count Parameter Result Qual Error ( 2 s) Batch: 0245332 FFSR U-234 1.1SE-05 9.SE-07 U-238 1.23E-05 1.0E-OS No. of Results: 2 Comments: Total Uneert( 2 s) MDC1MDA Work Order: L6GT01AC FORM II LCS RESULTS Report Unit Yield Report DB 10: 2.1 E-OS 1.4SE-07 UCI/SA 98% Ree Limits: 2.1E-OS 9.S2E-OS UC IISA 98%, Ree Limits: ---_.- TestAmerica Bias -{Resull/f.xpcclcdl-J as defined by A~SI XI3.3U. rptSTLRchLcs VS.2.7 Al002 T estAmcrica L aboratories, Inc. I~ SDG: 42004 Report No.: 44930 Expecll'd Keconry. EXPI:Ch'd lincerl Bias L6GT01CS 1.1SE-05 3.59E·07 102% 75 125 0.0 1.22E-05 3.7SE-07 101 % 75 125 0.0 Analysis, Prep Date 9/30/10 08:07 p 9/30/10 OS:07 p Date: 19-0cl-10 Aliquot Size 0.28 Sample 0.28 Sample Primary Detector ALP11 ALP11 FORM I SAMPLE RESULTS Date: 19-0ct-10 Lab Name: TestAmerica Lot-Sample No.: JOH310484-3 SDG: 42004 Report No.: 44930 CDC No.: Coliection Date: 8/25/20107:50:00 AM Received Date: 8/31/201010:30:00 AM Matrix: AIR FILTER Client Sample ID: R2 NYC FILTERS(5607,5608,5609& Denison Mine 2010 3rd atr Ordered by Client Sample ID, Batch No. Parameter Batch: 02<'5332 U-234 U-235 U-238 No. of Results: 3 Result FFSR 3.37E-02 1.SlE-03 3.S1E-02 Comments: Count Qual Error ( 2 s) B.BE-04 1.9E-04 9.0E-04 Total MDCIMDA, Rpt Unit, Uncert( 2 s) Action lev Lc Yield RstlMDC, CRDL(Rl) RsUTotUcert Analysis, Prep Date Work Order: l6CVC1AA Report 08 10: 9l6CVC10 5.3E-03 3.23E-05 Uel/SA 85% (1043.7) 9130110 OB:07 p 8.41 E-06 9.00E-1S (12 7) 3.2E-04 2.74E-OS Uel/SA 85% (5S.6) 9130/10 08:07 p 5.95E-06 9.00E-15 (10.2) 5.5E-03 3.93E-05 Uel/SA 85% (8927) 9/30/10 08:07 p 1.19E-OS 9.00E-15 112.7) .. --._-.---------------.. - Ratio U-2341238 = 1.0 TestAmerica MDC[MDA,Lc -Detection, Decision level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.00116 Sample 0.00116 Sample 0.00116 Sample ------ rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the MdclMda, Total Uncert,CRDL, or not identified by gamma scan software. VS.2.7 A2002 r cstAmcri...'J L.:1borJtorks. InL'. 10 Primary Detector ALP9 ALP9 ALP9 -i ~ ? q g' IT" g- ~ Q f c '-' Chain of Custody Record fAl-4IN(I@! Clisnt Temperature on Rec6ipr __ _ TestAmerica Drinking Water? Yes 0 No 0 THE LEADER IN ENVIRONMENTAL TESYlN(i Pro/Get /IIl!J(ISf1Cf -DSt8 Tetco ! Dean Kitchen i 8/26/2010 ~~m~~I~N~I~III!I,(l" r -~ ./ ;;'~ ,,-,. 0..; CtraitJ o(C:.'S!cd1' Number Address! ,--. -.." ---.--:;"..:..-".."..~-.-,., ."..:",--•. " '&/tiIPhOM NtJmbGr (At"" Codc}!Fax M.Prt.x;r Ll!b Numllc! '391 East 620 South Page ! of Ciry i . -_.-: I Sta,!O tzcCode_, Site ContaCt LsbCor.J;r.:f Ana!ysis (Artach list ff ;Amencan Fork . _Ut_. :.8,4.P_O~_. morospac9fsnO~D:j) . , Prok(;f NlJme ~t1ri Lcc;atio" IS:afcl Denison Mine 2010 3rd Quarter Can!rrJct/Pu.-coon Ordcr/Q,;::>!c No, C<rniiJ"IWaybi!l Nanue( .:., I AI' Containers B ,.,at!{x Preser/Stives -----------~ d, I • -~ Sample I.D. No. and DeSCtip~lOn 0 I T' _ _ ~.::, 8 _ -~ (C!1I'I18lners for sa-;;h s:1mple ma"J.' b'3 comtJlr.ed an em) Irr.e} z.e tme:li"(:~ ~ ~ ~ ~ ~ i t~~ -.. , -, '-=-p-. Rl Ba~~.':..use filter _ (S6CS)._ a~~_beaker .. ___ . 8/24/2010 ! 10:00 X I I I_ . -8/24/2010 -L ~:OO X I l ! , Rl NYC filters lS501,S602,~622) and beaker r R2 NYC_filters ISQ07,S5OS.S5091 and beaker , j I 8/25/2010 7:50 xii I-T _ J -, I i' I ~I ..;,.;<:" "j ~I ~ :::I i= ~ ~ ..,. ;g' , . III W'JA1 pil i; I "II il-itlf(f17C7 x ~ JLj,ql Oil('[ I \1 Spe:;;iallnstrtlctions/ COnditiOnSOf ~ • ~':://-I J.1{Jr -1. r/ Ir U-t '_ /, IU p-" "7:1/" I I .. J 1 I , I; 1 1 1 1 1 1 I IH.----I r -1-1 i ----j j -CRei:r,q;i~ ~ut -____ Li!~L~J:!<f-~6 ~~:,n / 6r{}(?J ~1 10.,. ,"'. I '~ 2. Fre/inoud:ed By 1 8:;"~'o I /Dcw~ to I nmQ D, ::J. R>:./lr.quiShccJ By I~-I tr~ 13. Ri:itiiW1:J By i I i);>.ts ! TIme Co:nmen!S When Complete Email to:DeanorPaul.tetco@tetco-ut.com brSTRIBUTION: WrlnE, Ri)lumed to-Ci~" ... ,ji!l Rtp()r~' CA,'\'A.':I'f -5!'3,Y$ ",i/;, tile S3mp/~: FINK· P.J;ld CCpr 0111 J~Vf?MiL' TestAmerica seiI1nf) 0 I. () -.2-r0 ·1 THE LEADER IN ENVIRONMENTAL TESTING eJe.II7'It-f-l(i) 0.1 _ -1 ~ ~. B Sample Check-in List V Lt?/V I-I-t~ i!;e~~..tl::3.11 c;(':) .. GM Screen Result, (out) (in) _____ lttitial .. [""'(b Client::tefCO SDG #: LtZtA2 i NA [1 SAF II: NA-(b Work Order Number:Qf21(E-10 VB51' Chain orCustody 11 _____________ _ Shipping Container 10: J'l,~ Air Bill II N~ Item 1 through 5 for shipping container only. Ini1ial appropriate response. I. Custody Seals on shipping container intact? vesl-{) No[ No Custody Seal r 2. Custody Seals dated and signed? yestVl No[ No Custody Seal [ 3. Chain of Custody record present'! ycs-Ol No [ 4. Cooler temperaturC: ___ NAV 5.Vonuiclllite/packing materials is NA [ 1 Wet [ 1 DryV Item 6 through 10 for samples. Initial appropriate rcspome. G. Number of samples in shipping container (Each sample may contain multiple bottleS):2~..t:2fZL~ 7. Sample holding times exceeded? NA v6 Yes [ 1 No [ 1 3~ 8. s;;gltCaSphe·ve: = / _.1..~. '~A't. hazard labels '-L---I I a~, __ custody seals ~IPpropria{C sample Jilbds 9. ,Sittlplcs afe: __ leaking -_Vingoodcolldition / nlJ.~""A /\ __ broken ~"J __ have air bubbles (Only for smnples requiring hend space) 10. Sample pH tuken? NA-f6 pH<2 [ J pH>2 [ 1 pH>9 [ Am0l11lt ofHN03 Addt.:d ____ _ Yc .. [t)J No [ 11. Sample Location, Sample Collector Listed? "" *for documentation only. No corrective action needed. 12. Were any anolllalies identified in sample receipt? Yes [ 1 Nrfl~ 1 13. Description of (lnolll£liies (include sample numbers): NA ( . //; AUhcr side ror additional COlTIJncnt:. .. ~~ Sample Custod'"L.......-~ ~A:: . Llate,&31 /~/20.6~~::1_· Client Informed on by Persoll contactcd, ______ _ [)Q No action necessary; process as is. Project Manager G'( ;)~ C)7)1C>!. O\i..--J LS·023, Rev. 10, 10/09 TeslAmcrica Laboratories. Inc. 14 APPENDIXD North Yellow Cake Scrubber Figure 1. Facility Schematic Representation Yellow Cake Dryer Baghouse Figure 2. Facility Schematic Representation Process Data (Retained by Denison Mines) D Facility: Denison Mines t a ~ y Stack Identification: North Yellow Cake Scrubber 1 +-0 ~1 i i p 13: Distance downstream from last disturbance, feet y: Distance of Sample Level to Ground, feet ____ -= Estimated Moisture, percent Estimated Temperature, °F __ ---':..:..:.. Estimated Velocity, fp m _'-"""' ____ _ Control Unit Type: Scrubber Number of Ports Figure 1. Facility Schematic Representation Process Type: Yellow Cake Processing Facility Denison Mines t CL ~ y Stack Identification: Baghouse 1~0 -+1 i , ~ a: Distance upstream from next disturbance, inches 57" 13: Distance downstream from last disturbance, inches 454" y: Distance of Sample Level to Ground, feet 65' 0: Stack Inside Diameter, inches 16" Estimated Moisture, percent 0-2% Estimated Temperature, of 125 Estimated Velocity, fpm 1,400 Control Unit Type: Baghouse Number of Ports 2 Figure 2. Facility Schematic Representation Pr ocess Type: Yellow Cake Processing Deni son Mine Proc ess Data So urce: No rlh Yellow Cak e Dale: <if ! ZA/ I,,) Snubber 1:low GPM Time II I 112 i1P '7i: c.) 0 ii' . '6-' I ,_,I, c1 '1 I 'Ii: 3<) 6-, ,cr-t c( <; '-/. I Ct: () 0 ,6"--,I( t L(. ') <-I· / C'{: ~\ '() ~),(t v-\· <\ (), I, to : 06 "';,'«-1 ,.\ ' tj '-f. c I O;~i) '(;1( H . '''I '1./ 114>:DO 1) <I-I. 'I, -+ i-f 1 L[ ?,O lr ' '1 i'-( , ~! L-f. I ('t, 0 " 6' '1 [ $-' C> L( , I 'l-$0 'i, "'/ I ,I ' 'i 1-( , () 1> () 1,.) II · k 1.5 , () 1.-(, 0 I} !:o f), ee-1'1, "'/ L{, 0 1'1 00 if, J;' ( '{'Ir L-{ , I 1,( '}o (6 ' <,-l'1. ~-c.{, \ I s-ut:> \ '-I 'f \..{,O r '\( ':'-3() \('\{ \ ~\, '\ '--\'U l~ o t) '6 . '{ \ ~l "i ,-I· D , (, >-(l b-Y-l '-l ' (-'-/ t_( . c) Ir oU b-'y \'1 , c\ LI ' () T\./,) ,) De ni son Mill e Proces s Data I Source: No rth Yellow Cake Date: 'I t ?--7f t6 Scrubber Flow U I'M Time Iii 112 tiP ?f .,) 1'(. I '"I. ! , <:( 0 ", I Y 30 ~+ I '1-1~ el· I ( '11" ~ + -n'l l~ .l "'" "'" " "', 30 8· 1) I't, '0 'i '/ 10 1I (..') c"..y,-Ilf· Y '-I . ( I f.) 30 Y ~' ILl · Y 4·(/ , 1 (I (} ~ . <1-(<..( r-C(. (; l\ 30 'ii . c( i L.(. 'if r'-{· 0 I Z (,0 y '¥' Ie.{ '1> '-h~ - ,'L 30 Cd-'i I L(, 4 (j. () I '> (6 ' "Y I c{·1 '-1.0 (.>0 I ') 30 ~ . ~f I L{. G. cf. 0 L« 0" 9;.)' L l( '? o.{. ? --t'l ,I L> Y, ~. I '1, <0' L(. ,-I. <>0 ~.~ t-1 . /-J-'-{. I , ,-¥~ '"~ <.( y I L(. ¥' I..{ . e:- 'il u '" ~.~ \L\.C.\ L,( . l\ I~ sO Cd ' y \ ~\ . "I vi-t:> -I -r " ,) .- -- APPENDIX E Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature sensors were carried out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 3 Schematic of Method 5/114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-test Dry Gas Meter Calibration Data Forms Type S Pitot Tube Inspection Data Sample Box Temperature Sensor Calibration E Schematic of Method 5/114 Sampling Train W. ii1 m Duct fa w~'1 Suppon Chain Th v.-,-, . elm-'.-iOC:.::u:!:p:::le:.--~j ; l Supoort T t. \ Kl . .' raeA. \ Kl --; Heated " ~. L -P'-obe ............... ~ ;',1"1;' . _ sampling. Probe I ;C'a~ n~1 (D Thermometer Vacuum /<t~ .... ..:, _.. r l ' mpmgerj .'\') G .' w-n T"""--'-Z'_J-..." _... _ Filter Bo'" I ::';: Y',' uage / ' . ----' \ ' ., Pitot .~,( ~ "'n , __ L Bo,;: 1 ___ "":' Check Valve :It-I ~. _J Sealed Flan.e //., TJ ' I Vacuum ---. / ,. __ ~ Manometer _ ~me •• c' L-,j Main Exit 'I I 1 I I ~~ Melermg ! fA' T h ": Valv-: Console I t IT Ig t '. ! By-pass: ... f ___ ~ IPumo I .-'-::::., Valve Figure 3 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical onfices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated. METER SERIAl#:~ CRITICAL ORIFICE SET SERIAL #:~ EQUIPMENT 10 #: K' TESTED TEMPERATURES of INITIAL FINAL 25.70 ELAPSED AVG(Pbot) 25.70 2010 Pre-Calibration IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECAUBRATEO 1 FACTOR VACUUM I DGM READINGS (Fn I AMBIENTI OGM INLET I OGM OUTLET I OGM TIME(M1N) I OGM .~ II (1) I (2) I (3) IV_~ON '%)~ I ORIFICE# I RUN# (AVG) (inHg) I INITIAL I FINAL I NET (V.,) I INITIAL fiNAL INITIAL Fltw.. AVG e (in H~) V .. (STO) Va (STD) y G G G 2 3 2 3 2 3 0.8137 0.8137 0.8137 0.5317 0.5317 0.5317 0.3307 0.3307 0.3307 13 164.506 13 169.770 13 175.087 12 197.702 12 210.703 12 216.011 12 181.2020 12 186.454 12 191.722 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 169.770 175.087 180.451 202.995 216.011 221.324 186.454 191.722 196.990 5.264 5.317 5.364 5.293 ~308 5.313 5.252 5.268 5.268 7. 7. 7. 7. 7. 7. 7. 7. 7. 63 68 68 75 75 '" 81 82 82 82 82 82 80 81 81 82 82 81 86 90 90 100 100 103 92 95 95 97 97 98 92 95 95 96 96 92 76.75 83.25 89.25 87.50 89.00 89.75 87.00 88." 87.75 §oo §.oo 5.00 3.00 5.00 3.00 §.50 7.50 7.50 §.20 1.20 1.20 §AO 0.40 OAO ~ 1:illI 4.4679 4.4003 4.4007 4.3989 4.3603 4.3616 4,3675 4.5261 4.5261 4.5261 AVG: .A363 4.4363 4.4363 AVG: 4.4147 4.4147 ~ AVG: 1.009 1.011 1.013 1.011 1.008 1.008 1.009 1.008 1.:D.Jl 1.012 1.011 1.012 0.05 -0.20 0.15 The fotlwing equations are used 10 cabJlale the slandard ~lunes of air passed through the DGM, V", (Sid). and lhe critical OrifICe, Va (Sid), and lhe DGM caibration factor, Y. These equaoons are automali:;aly cabJiated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 1.010 (1) (2) (3) Vm(>lJ) = Kl • Vm. Pbar + (&H II 3.6) Tm Pbar .0 Vcr(s",,/) = K ' • ..jT;;;j; = Net \'QIume of gas sample passed through DGM, corrected to standard conditions K,:: 17.64 "R/in. Hg (English), 0.3858 "KImm Hg (Metric) T .... Absolute OGM avg. temperature ("R. -English, ~ -Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T _:: Absolute ambient temperature ("R -English. "K -Metric) K':: Average K' factor from Critical Orifice Calibration Ver,,,,I) y = -- Vm(.,J) = DGM calibration factor AVERAGE 6.HO :1 1.571 ( 0.75 Q )2 AH (V",(std») V",(std) V .. AHO = Temperature Sensors Reference In Out OF OF OF 33 34 34 67 66 66 121 120 120 PRE Console #6 Calibration 2010 1.755 1.734 llll 1&Q! 1.600 1.597 1.:m 1.376 1.378 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report). for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YEllOW cens are calculated. METER SERIAL #:~ DATE:11I12121J11J I CRlTlCAl ORIFICE SET SERIAL #:~ EQUIPMENT 10 #: K' TESTED TEMPERATURES ·F FACTOR VACUUM I OGM READINGS (FT', I AMBIENT I DGM'NLET, I DGMDUTl~1 I ORIFICE" I RUN # (AVG) (in Hg) I INITIAL I FINAL I NET (V..) I INITIAL fiNAL INITIAL FINAL o G G 2 3 , 3 2 0.8137 0.8137 0.8137 0.5317 0.5317 0.5317 0.3307 0.3307 0.3307 12 565.308 12 571 .918 12 578.535 12 528.501 12 534.214 12 539.920 12 547.8020 12 553.G49 12 558.331 USING THE CRITICAL ORIFICESAS CALIBRATION STANDARDS: 571.918 578..535 585.208 534.214 539.920 545.630 553.049 558.337 563.648 6.610 6.617 6.673 5.713 5.706 5.710 5.247 " .. 5.311 n n 72 74 74 7. 72 n n 90 92 92 90 90 .9 77 ., •• 92 92 93 92 93 93 94 93 .. 90 90 90 91 90 91 9' 91 92 ., 7. 84 •• 84 .9 90 .. 93 INIT1AL DGM AVG 91.75 92,' 93.15 90.00 ",50 91.00 80.00 85.00 89.SO FINAL 25.67 ELAPseD TIME (MIN) e §'OO 6.00 6.00 8.00 8.00 8.00 12.00 12.00 12.00 2010 Pre-Calibration Console 7 AVG(PI>o,) 25.67 IDGM':1 1(1),1 (In H20) V",(STD) 2.65 2.65 2.65 1.12 1.12 1.12 0.41 0.41 0.47 M§2!! ~ 5.5012 4.n13 !.Z11! 4.7103 ~ ~ ~ IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 1 (2) I (3) I VAR~~ONI" ~ V«(STD) y ~ 5.4352 5.4352 AVG= ~ 4.1265 4.1265 AVG:: 4.4179 4.4179 ~ AVG= 2&2! 2&2! MM 20m ~ 1&ll 1&ll L2n ~ 1.004 ~ ~ ~ ~ 2M 1..m ~ ~ 1.492 >A90 ~ Ul2 1.624 1&!Q. The lolk>wlng equations are used localculale the standard volumes 01 air passed through the DGM. Vm (std), and the critral orifi:e, Va (Sid). and the DGM calibration factor. Y. These equations are aulomaticallycalculaled in the spreadsheet above. AVERAGE DRY GAS METER CAL1BRATION FACTOR, Y = I 1.000 (1) (2) (3) Vmt.,I) = K[. Vm-Pbar + (aH /13.6) Tm Pbal'·0 Veri .. ") = K'· JTa;;b = Net volume of gas sample passed through DGM, corrected to standard conditions Kl :: 17.64 "RIin. Hg (English). 0.3858 "KImm Hg (Metric) T m = Absolute DGM avg. temperature ('R -English. "K -Metric) = Volume of gas sample passed through Ihe critical orifice, corrected to standard conditions T _:: Absolute ambient terT1)erature ("R -English, ~ -Metric) K'. Average K' factOf from Critical Orifice Calibration VC'i.tJ) y = --= DGM calibration factor Vmt"/, AVERAGE.6HO=1 1.538 AHO = (0.759)' t.H (Vmlstd») Vcr(std) Vm Temperature Sensors Reference In Oul OF 32 72 120 OF 33 73 120 OF 32 72 120 PRE Console #7 Calibration 2010 r: ." 'is QuulllJ-~n·lu·R('lIIlultlJ ~T~'i ~~~r-J r METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operatmg range. 2) Record barometrrc pressure before and after calibration procedure. :S) Kun at tesleo vacuum (Trom untlce l,;alloratlOn KepOrt), rot a penoa or time ne--...essary to aChieve a minimum total volume of 5 cubic feel. 4) Record data and information in the GREEN cells, YEllOW cells are calculated. METER SERIAL #:1-==-1 CRITICA.l ORIFICE SET SERIAL #:L-_='--' EQUIPMENT 10 *: K' TESTED TEMPERATURES "F FINAl 25.28 ELAPSED AVG (P~ .. I 25.28 Denison Mines IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECAUBRATED 1 FACTOR VACUUM I DGM READINGS IF"") I AMBIENTI OGM INLET I OGM OUTLET I OGM TIME (MIN) IOGM·:I I (1) I (2) I (3) I VARIA~ON{~"~ I ORIFICE #-I RUN # (AVG) (in Hg) I INITIAL I "NAL I NET (V.) I INiTlAL FIN.\l INITIAL FJHA!. AVG 0 (in H20) V",ISTO) Vct(STD) V G G : 0.5317 0.5317 0.5317 0.6808 0.S808 0.S808 14 14 14 11 11 11 57.005 62.051 67.131 72.685 77.730 82.865 62.051 67.131 72.229 77.730 82.8S5 88.232 5.046 5.080 5.098 5.045 5.135 5.367 77 75 78 85 77 78 " " 77 " .4 " 77 8S " 103 77 87 90 108 77 90 91 114 92 " 104 108 114 117 82.5 87.75 92.25 95.75 99.75 103.00 7.25 7.25 7.25 §.50 5.50 5.15 1.20 1.20 1.20 2.10 2.10 2.10 llill ~ um 4.0752 i.1lli !J.ill 4.2065 ~ ~ AVG: 4.0860 ~ 4.2717 .1.Q1Q 1JU1 1.9.1! !:.2.!1 .1QQ1 0.992 0.998 0.79 D:§~ : I I I I I I ::: § § AVG" ~ ~.79 AVG", USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: The fol.-ow,r.g e~!liitons are used to caicula:e !he sia1da"d VO!umes of air passed :hrough the OGM, V",. (sid), ana !he critical onf:ce, V., (Sll;l), ar.d Ihe DGM ca!.ibratioo fact.or, Y. These eq!Ja'JOOs a'e automatically calcu'aled in me spreads'leet at>Yle AVERAGE DRY GAS METER CALIBRATION FACTOR, Y '" r-1~006:J (1) (2) (3) /' -K d ' .Pbclr +(MflI3.6) m",." -I m Till Pbal' .. 0 J 'cr: ... I, = K'· -,Fia;;;;; '" Net volume of gas sample passed through DGM, corrected to slandard conditions K, .. 17.64 OR/in Hg (English), 0 3958 'Kfmm Hg (Metric) T", :r:: Absolute DGM avg temperature ('R -English OK _ Metric) :: Volume of gas sample passed through the critical orifi~, corrected to standard conditIons T,."., '" Absolute amcienl temperature ("R -Engijsh, 'K -MeIne, K'::: Average K' factor flom Clitical O:lrlCe CaJibfati:)f'J r rcr,,,;, VIII,,,J. :::: DGM callbrabon factor AVERAGE ;H® "I 1.679 ) 6.H~ '" (0.75 e )' 6H (Vm(std)) Vc,(std) v", Temperature Sensors Reference In Out OF 33 57 121 OF 34 56 120 OF 34 65 120 Post test Console #5 !.ill 1.639 ~ 1112 !:ill 1.ill METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 8M M"'i'gW"& 'l!~-~i.-'-'-.!; E ··· 1) Sell!ct three critical orifices to calibrate ti;e dry gas meter which bracket the expected opernbng ran;e. 2) Record barometric pressure before ami after calibration procedure. 3) Run at tested vacuum (from Orifice Cattbration Report). for a period of time necessary to achieve a mimmum total yolume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated. INITIAL METER SERJAllI:c=J CRITICAL ORIFICE SET SERIAl *:~ EQU!PMENT!O II: K' TESTED TEMPERATURES of ii) ;.'" > ,"'t' I ; Facility Denison Mines F1NAL AVG (P~) 25.39 25.39 ELAPSED IF Y VAR!ATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 1 FACTOR VACUUM I OGM READINGS (FTl) I AMBIENT I OGM INLET. I DGM OUTLE~ I DGM TIME (MIN) r::ll (1) ,I (2) I (3) I VARlA~ON(~J ~ I ORIFICE # I RUN /I (AVG) (in Hg) I INITIAL I FINAL I NET (V.) I INITIAl. FINAl. lNlT~ FINAl. AVG • (in HID) V", (STD) v .. (STO) y 0.6808 12 673.872 679.086 0.6808 12 679.086 684.320 0.6808 12 684.320 689.515 G : 0.5311 " 651.462 662.550 0.5311 " 662.550 661.646 0.5311 ,. 661.646 612.765 5.214 5.234 5.255 5.088 5.096 5.119 80 80 .0 .0 .0 .0 82 B4 B4 •• •• 88 78 7. 7. 79 79 ., 88 92 92 95 OS " 78 .0 80 ., ., .7 86.5 89.25 91.15 78.50 80.00 82.50 5.75 5.75 5.75 5.75 5.15 5.15 1.25 1.25 1.25 2.10 2.10 2.10 2.10 2.10 2.10 1.25 1.25 1.25 1.25 1.25 1.25 4.3015 ~ 4.2~1 4.2495 4.2444 4.2439 4.2184 4.2184 4.2784 AVG", 4.2130 4.2130 ~ 0.995 0.996 0.996 0.996 0.991 0.993 Q.i21 0.11 G D :EE§ : I I I I I I:: § § AVG' 0.992 = AVG= USING THE CRITICAL ORIFICeS AS CAl!9RATlON STANDARDS: The foJlo'>\"ir.gBq!Jalionsara use:]" to calculate tlla standar(! vol!Jmesof air pa~d througn the DGM, V .. {sId), and Ine cmcal entice, Va {sid), and the DGMcalibraoor. f~or. Y. These equations are .;utomatica:tycabJlated In the sprei'ldsheetabove AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = [ 0.994--, (1) (2) (3) //m{ul' to KI * I'm"' ?b:lr + (~!~113.6) Tm I'cr"." :: Pbar. ~ K '. --:.;-f"amb = Net volume of gas sample passed through DGM. correcle::l to standard conditions K, '" 11 64 'RI,n Hg (English). 0 3353 OWmm Hg (Mem::) T ... AbsclUle DGM avg temperature C'R -Engb$h."K -MetrJ:j = Volume of gas sample passed through the critical orifice. corrected 10 standard condilions T _" Absolute "mOlent terr.perature ('R _ English. OK -Metric) K''' Aver3~ K' fa:;tor from Cfltl~l Oulice Ca:lbral:on Vcr,.",) }'= --- Vm,,<o11 = DGM calibration factor AVERAGEdH.=1 1.74 6Hft = ( 0.750 )' dH (V",{std)) Vc,(std) V", ill ill ill ill ill ill POST Conscle #7 Calibration 2010 Typc S PilOt Tubc Inspectioll Data ,~ /)1'O&~lL_i!l ~p .. , "cc-_,_'..:.j .c;f_I.LJ ___ '" , "(-:,') '" r!1 < 10" ((1 < 10" a, -_-,,:0 __ _ CIJ "' __ -'-___ _ ~,------ z ~O 125 in z-' 00 \:> W ~OO)1 25 in w '" 'OD B W > 3 I1lchcs W ... 10 1/ .... Z > )/·\ inch Z'" l[e ~" """"--4> " , ... ~...... . -.~ ......... ..--I-"i:---__ y ~ 3 im:hl~s The pilot lube 11,,'cl:; thc SIX-ciflcalions for a ("lllbrlllion (actor of 0 S.p ___ _ T C1I1\x:raLlirc Sensor Call1.lr;lllon Referencc' ? :,' Temperature r em );~r;lIurc r~ll1pcr"llJr<". Sour.:e Rd l'fCnCC ScnSQr /)i{fcr.;:ncc '.' >-(M{'(lium) f'F) ("I') (''I') AIR vS Ip fo z.. Pwbc Conlinuitv 7 --7 \( e. ') 1'11':\\ Check 201.1{ ---} '/ e..S 1.S"'i AIR (, S lor I ICE WATER 3 '1 'b '-l if StOlek tlOIL WATER 'Z. ,,'j 201. 7- ~II.1CONE Oil in. in. in. in. Type S '·itot Tulle Inspection n ala I'itot T!:bc Jd~lllificatioll' _,,2:... -'7_-_..:1.7::.-______ _ • OF ' :3"'"/.) ,n II" = <J'U III. PI!'" . C( I_{ ~~ '" ((I < I()~ {II"" (.12 < 10· (J;~"" 2 Ill'" --- Z :> 0 125 ill. Z .0 1:( , ' __ -, ___ m, IV w s003t25m. w '" __ ,_,_-,_1_-..;',-_,,, W > 3 iuclws in. Z> 3!·1 inch Z -______ in. y ~ 3 mdn:s " 'Ii y ,-, __ '_LI'J.::s __ in Till! pilot lithe rn ... cts the spccirl'-ations ror il call1lr Ll!\)Il fL":lnr ufO S .. P 'j.e,5 .. TCIlle£I:IIUrC Sensor Cahbl.l\ioll Refcrcllcc , <> T cmpclatLJr,~ TCr11jl(~ralurc TCnljlClaturc S()Uf~t Refereuce Sensor DlIli;rl!lI(;c . (Medium) ("F) n) (OF) AlII. (p ~I-(" l -ID " I'rohc ContinuilV c.~U(._ 'i-e.';> Ikal Check 248 --~ ~(..:,> 7.(,0 AIR (, B b :}-I ICE WATER .~ <, '3 ~'> ,0- Stack DOlL wt\TEI~ -/..0,:) Lo" ,0" SIUCONEOIL TETCO Sample Box Temperature Sensor Calibration Dale: 1113/2010 Calibrator: Mike McNamara Reference, Omega CL3512A ore Temp. Diff. Thermocouple " ~~ Unit ID Source fl S~?:)or or Result Location ('F) (oF), PfI'-, Oven Water 33 32 I Water 203 204 I A Probe Out Water 33 32 I Water 203 203 - Impinger Out Water 33 32 I Water 203 202 I Oven Water 33 32 I Water 203 204 I B Probe Out Water 33 32 I Water 203 203 - Impinger Out Water 33 34 I Water 203 202 I Oven Water 33 33 - Water 203 203 - C Probe Out Water 33 31 - Water 203 202 I Impinger Out Water 33 34 I Water 203 202 I Oven Water 33 32 I Water 203 203 - D Probe Out Water 33 32 I Water 2~ 2Q2 - Impinger Out Water 33 34 I Water 203 202 I Oven Water 33 33 - Water 203 204 I E Probe Out Water 33 33 - Water 203 203 - Impinger Out Water 33 34 I Water 203 201 2 Oven Water 33 33 - Water 203 204 I F Probe Out Water -33 32 I Water 203 203 - Impinger Out Water 33 33 - Water 203 202 I I Impinger Out G I Water 33 34 I Water 203 201 2 Impinger Out H Water 33 34 I Water 203 202 I Impinger Out I Water 3 3 - Water 2 )3 21 - Impinger Out J I Water 3 - Water 2)3 21 I APPENDIXF The testing followed the same procedures as outlined in previous protocols and tests at this facility. Prepared for: FOURTH QUARTER RADIONUCLIDE EMISSIONS TEST CONDUCTED AT DENISON MINES CORPORA TlON NORTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE GRIZZLY BAGHOUSE BLANDING, UTAH October 19, 2010 December 7-8, 2010 by: TETCO 391 East 620 South American Fork, UT 84003 Phone (801) 492-9106 Fax (801) 492-9107 fax Denison Mines Corporation 6425 S Hwy 91 Blanding, Utah 84511 Date of Report: Febrnary 7, 2010 CERTIFICATION OF REPORT INTEGRITY Technical Emissions Testin g Company (TETCO) certifies that this report represents the truth as well as can be derived by the mcthods employed. Every effort was made to obtain accurate and representati ve data and to compl y with procedures set forth in the Federal Register. Dean Ki (chen Reviewer: ~~ Date: ________ -LJ.-_-~Z<__~_/~/_ j ~ I~ Mike McNamara Rcviewer:---"-""1i#1L'-'------¥---'-~ __ Date: ___ L---'--h-'-'-(-'.\..I( _____ _ ii TABLE OF CONTENTS Introduction Test Purpose ...................................•...............•........ I Test Location and Type of Process .......................................... I Test Dates ............................................................. I Po llutants Tested and Methods Applied ...................................... I Test Participants ......................................................... 2 Deviations From EPA Methods ............................................. 2 Quality Assurance ....................................................... 2 Summary of Results Emission Results ........................................................ 3 Process Data ............................................................ 3 Description of Collected Samples ........................................... 3 Discussion of Errors or Irregularities ......................................... 4 Percent Isokinetics ....................................................... 4 Source Operation Process Control Devices Operation .......................................... 5 Process Representativeness ................................................ 5 Sampling and Analysis Procedures Sampling Port Location ................................................... 6 Sampling Point Location .................................................. 6 Sampling Train Description ................................................ 7 Sampling and Analytical Procedures ......................................... 7 Quality Assurance .......................•.............••................ 7 Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence iii LIST OF TABLES Table I Measured Radionuc1ide Emissions .......................................... 3 II Percent Isokinetics ....................................................... 4 III Sampling Point Location .................................................. 6 IV Complete Results, North Yellow Cake Scrubber ...................... Appendix A V Complete Results, Yellow Cake Dryer Baghouse ...................... Appendix A VI Complete Results, Grizzly Baghouse ............................... Appendix A LIST OF FIGURES Figure I Facility Schematic Representation North Yellow Cake Scrubber .......... Appendix D 2 Facility Schematic Representation Yellow Cake Dryer Baghouse ......... Appendix D 3 Facility Schematic Representation Grizzly Baghouse ................... Appendix D 4 Schematic of Method 51114 Sampling Train .......................... Appendix E iv INTRODUCTION Test Purpose This test project was conducted to determine the total radionuclide emissions from the North Yellow Cake Scrubber, Yellow Cake Dryer Baghouse, and Grizzly Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dscl). These tests were for U-Nat and Th-230 on the Grizzly Baghouse and U-Nat, Th-230, Ra-226, and Pb-21 0 on the North Yellow Cake Scrubber and Yellow Cake Dryer Baghouse. Test Location and Type of Process Denison Mines (USA) Corporation is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Dryer Baghouse. The Packaging enclosure also discharges into the Dryer Baghouse. The North Yellow Cake (NYC) dryer was the only operating dryer at the time of the test. The South Yellow Cake Dryer is currently not operational. The Grizzly Baghouse serve as the main dust control device for the raw ore unloading and conveying to the processing building. Stack schematics are shown as Figures 1 though 3 in Appendix D. Test Dates One run was completed on the Grizzly Baghouse October 19,2010. One test run was completed on the NYC Dryer December 7,2010 and one run on December 8th• One run was completed on the Dryer Baghouse December 8,2010. Pollutants Tested and Methods Applied The tests were a determination of radionuclide emissions in accordance with EPA Method 5/114. Test run filters and front wash residues were sent to Test America located in Richland, Washington for radionuclide analysis. Test Participants Test Facility State Agency TETCO Ryan Palmer None Doug Olsen Mike McNamara Deviations From EPA Methods None Quality Assurance Joseph Kitchen Kawai McNamara Testing procedures and sample recovery techniques were according to those outlined in the Federal Register and the Quality Assurance Handbookfor Air Pollution Measurement Systems. 2 SUMMARY OF RESULTS Emission Results Table I presents the findings of the test in Curies per dry standard cubic foot. Tables IV-VII in Appendix A have more detailed information. Table I. Measured Radionuclide Emissions North Yellow Cake Yellow Cake Dryer Grizzly Baghouse Run # Scrubber Baghouse pCi/dscf pCilhr pCildscf pCi/hr pCi/dscf pCilhr 407.9 2.654E+07 29.9 3.3 20E+06 0.002 1.859E+02 2 354.9 2.33 2E+07 AVE 381.4 2.493E+07 29.9 3.320E+06 0.002 1.859E+02 Process Data The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow, pressure drop readings (L'.p) were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (L'.p) were recorded and are found on the test run sheets. Production data will be submitted by Denison Mines. Description of Collected Samples The test fi lters for the North Yellow Cake Scrubber were heavily covered with a white or pinkish white colored particulate. The front washes were clear in appearance. The test filters for the Yellow Cake Dryer Baghouse were lightly colored with a tan colored particulate. The front wash was clear in appearance. The test filters for the Grizzly Baghouse were had no visible particulate. The front wash was clear in appearance. Discussion of Errors or Irregularities 3 None Percent Isokinetic Sampling Each of the tests were isokinetic within the ± I 0% of 100% criterion specified in the Federal Register. They also meet the Utah State Department of Environmental Quality, Division of Air Quality specification of isokinetic sampling point by point. Isokinetic values for each test run are presented in Table II. Table II. Percent Isokinetic Sam lin Run # 2 North Yell ow Yellow Cake Cake Scrubber Dryer Baghouse 101 97 4 98 Grizzly Baghouse 100 SOURCE OPERA nON Process Control Devices Operation All process control devices were operated normally. Recorded scrubber water flow, pressure and baghouse ~p readings were recorded and are found on the test run sheets or in Appendix D. Process Representativeness The facility was operated normally. Production data was retained by Denison Mines. 5 SAMPLING AND ANALYSIS PROCEDURES Samplin g Port Location The inside diameter of the North Yellow Cake Scrubber stack is 18.0 inches. The two, four-inch diameter sample port are located 6.3 diameters (9.5 feet) downstream from the last disturbance and 6.3 diameters (9.5 feet) upstream from the next di sturbance. Figure I in Appendix D is a schematic of the stack. The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch diameter sample ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 2 in Appendix D. The inside diameter of the Grizzly Baghouse stack is 18.75 inches. There are two, three-inch diameter sample ports located 2.56 diameters (48 inches) downstream from the last disturbance and 1.31 diameters (24.5 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 3 in Appendix D. Sampling Point Location Table III shows the distance of each sampling point from the inside wall according to EPA Method I. Each point is marked and identified with a wrapping of glass tape and numbered. These points are determined by measuring the distance from the inside wall. Distance . from Inside Wall Sample Point 0.58 0.70 0.50 2 1.89 2.34 1.26 3 3.49 4.74 2.21 4 5.81 11.26 3.32 5 12.19 13.66 4.69 6 14.51 15.30 6.68 7 16.11 12 .08 8 14.06 9 15.43 10 16.54 11 6 Sampling Train Description To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-5/114 were followed. All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent interference of the sampled gas and particulate. The stack analyzers used to conduct Methods 1-5/114 are constructed to meet the specifications outlined in the CFR. The temperature sensors are K-type thermocouples. Heater, vacuum and pitot line connections have been designed to be interchangeable with all units used by the tester. A 316 stainless steel probe liner was used for the tests. Figure 4 in Appendix E is a sketch of the Methods 5/114 sampling train. Sample boxes were prepared for testing by following the prescribed procedures outlined in Methods 5/114. Sampling and Analytical Procednres All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 5/114. Quality Assu rance All equipment set-up, sampling procedures, sample recovery and equipment calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbook/or Air Pol/ution Measurement Systems. 7 APPENDIX A: Complete Results and Sample Calculations B: Raw Field Data C: LaboratOlY Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence 8 APPENDIX A Table IV Complete Results, North Yellow Cake Scrubber Table V Complete Results, Yellow Cake Dryer Baghouse Table VI Complete Results, Grizzly Baghouse Nomenclature Sample Equations A NYC Scrubber TABLE IV COMPLETE RESULTS DENISON MINES CORPORATION, BLANDING, UTAH NORTH YELLOWCAKE SCRUBBER EXHAUST Symbol DescriEtion Dimensions Run#1 Run #2 Date 1217110 12/8/10 Filter # 5677 5679 Begin Time Test Began 7:58 7:50 End Time Test Ended 18:03 16:03 Pbm Meter Barometric Pressure In. Hg. Abs 24.60 24.65 6H Orifice Pressurc Drop In. H2O 0.916 0.969 Y Meter Calibration Y Factor dimensionless 1.010 1.010 Vm Volume Gas Sampled--Mcter Conditions " 297.727 304.173 Tm Avg Meter Temperature OF 96.4 94.0 Y6P Sq Root Velocity Head Root In. Hz{) 0.2315 0.2319 Wtwe Weight Water Collected Grams 638.6 653.9 Tt DurationofTest Minutes 480 480 C, Pilot Tube Coefficicnt Dimensionless 0.84 0.84 Do N07.zle Diameter Inches 0.3810 0.3920 CO, Volume % Carbon Dioxide Percent 3.50 3.30 0, Volume % Oxygen Percent 16.20 16.10 N,&CO Volume % Nitrogen and Carbon Monoxide Percent 80.30 80.60 Vmstd Volume Gas Sampled (Standard) ."r 235.260 241.922 Vw Volume Water Vapor .or 30.110 30.83 1 Bw s (measured) Fraction H20 in Stack Gas (Measured) Fraction 0.113 0.113 Bw S (saturatcd) Fraction H20 in Stack Gas (Saturated) Fraction 0.110 0.104 Bw, Fraction H20 in Stack Gas * Fraction 0.110 0.104 X, Fraction of Dry Gas Fraction 0.890 0.896 M, Molecular WI. Dry Gas lbllbmol 29.21 29.17 M, Molecular WI. Stack Gas lbllbmol 27.98 28.01 %1 Percent lsokinetic Percent 100.9 97.0 AVG T, Avg Stack Temperature "F IIIJ 109.6 110.5 A, Stack Cross Sectional Area Sq. FI. 1.767 1.767 Po Stack Stalic Pressure In. H20 -0.045 -0.045 Pb, Sample Pon Barometric Pressure In. Hg. Abs 24.53 24.58 P, Stack Prcssure In. IIg. Abs 24.527 24.577 Q, Stack Gas Volumetric Flow Rate (Std) dscfm 1.08E+03 1.I 0E+03 1.09E+03 Q, Stack Gas Volumetric Flow Rate (Actual) cflll 1.61E+03 1.61E+03 1.61E+03 V, Velocity of Stack Gas fpm 9.1OE+02 9.09E+02 9.10E+02 Curies Radionuclides per sample pC; 95962.1 85864.8 ** Crad Concentration of Radionuclides pCildscf 407.898 354.927 381.412 ERrad Emission Rate of Radionuclides pCi/lir 2.654E+07 2J32E+07 2.493E+07 * If the measured moisture content is greater than the saturated moisture level (supersaturated), the saturated moisture value will be used in all calculations (40 CFR 60, Method 4, Section 12.1 .7). Symbol Date Filter # Begin End Pbrn ~H Y Vm Tm ,j~P Wtwe T, Cp Do CO, 0, N,&CO Vmstd Vw Bw, Xd Md M, %1 T, A, PG Pbp P, Q, Q, V, Curies Crad ERrad • TABLE V COMPLETE RESULTS. PM DENISON MINES CORPORATION YELLOW CAKE DRYER BAGHOUSE Descri~tion Dimensions Run #1 Date 12/811 0 5676 Time Test Began 9:32 Time Test Ended 11:34 Meter Barometric Pressure In. Hg. Abs 24.65 Orifice Pressure Drop In. H20 0.969 MeterCalibration Y Factor dimensionless 1.002 Volume Gas Sampled .. Meter Conditions " 79.208 Avg Meter Temperature 'F 76.3 Sq Root Velocity Head Root In.lhO 0.4397 Weight Water Collected Grams 10.9 Duration of Test Minutes 120 Pitot Tube Coefficient Dimensionless 0.84 N01..z1e Diameter Inches 0.2760 Volume % Carbon Dioxide Percent 0.00 Volume % Oxygen Percent 20.90 Volume % Nitrogen and Carbon Monoxide Pcrccnt 79.10 Volume Gas Samplcd (Standard) d",r 64.561 Volume Water Vapor .or 0.514 Fraction H20 in Stllck Gas Fraction 0.008 Fraction of Dry Gas Fraction 0.992 Molecular WI. Dry Gas lbllbmol 28.84 Molecular WI. Stack Gas lbllbmol 28.75 Percelllisokinctic Percent 97.9 Avg Stack Temperature 'F 76.7 Stack Cross Sectional Area Sq. Ft. 1.396 Slack Static Pressure In.H~ -0.2 1 Sample Port Barometric Pressure In. Hg. Abs 24.58 Stack Pressure In. Hg. Abs 24.565 Stack Gas Volumetric Flow Rate (Std) dscfrn 1.85E+03 Stack Gas Volumetric Flow Rate (Actual) din 2.31E+03 Velocity of Stack Gas fpm 1.65E+03 Radiolluelides per sample pCi 1933.6 • Concentration of Radionuclides pCildscf 29.9498 Emission Rate of Radionuclides pCiIhr 3.320E+06 Values below the detection lim it are not included. Dryer Baghouse Grizzly TABLE VI COMPLETE RESULTS, PM DENISON MINES CORPORATION GRIZZLY BAG HOUSE Symbol DescriEtion Dimensions Run #1 Date Dale 10/19/10 Filter # 5642 Begin Time Test Began 9:25 End Time Tesl Ended 17:48 Pbm MeIer Baromelrie Pressure In. IIg. Abs 24.50 IIH Orifice Pressure Drop In. H20 1.054 Y Meter Calibrntion Y Factor dimensionless 1.000 Vm Volume Gas Sampled--Melcr Conditions ,r 323.222 Tm Avg MeIer Temperature 'F 86.7 VIIP Sq Root Velocity Head Roolln. H2O 0.2311 Wtwc Weight Water COllected Grams 60.7 T, DurntionofTest Minutes 480 C, Pitot Tube Cocfflcient Dimensionless 0.84 0, Nozzle Diameter Inches 0.3765 CO, Volume % Carbon Dioxide Percent 0.00 0, Volume % Oxygen Percent 20.90 N,&CO Volume % Nitrogen and Carbon Monoll:ide Percent 79.10 Vms1d Volume Gas Sampled (Standard) dscf 256.426 Vw Volume Waler Vapor "r 2.862 Bw, Fraction H20 in Slack Gas Fraction 0.011 X, Fraction of DI)' Gas Fraction 0.989 M, Molecular WI. 01)' Gas Ibllbmol 28.84 M, Molecular WI. Stack Gas lb/lbmol 28.72 %1 Perccntisokinetic Percent 100.0 T, Avg Stack Temperature 'F 79.3 A, Stack Cross Sectional Area Sq. FI. 1.917 Po Stack Static Pressure In. H2O -0.06 Pb, Sample POll Barometric Pressure In. Hg. Abs 24.47 P, Slack Pressure In. Hg. Abs 24.466 Q, Slack Gas Volumelric Flow Rate (Std) dscflll 1.32E+03 Q, Slack Gas Volumelric Flow Rate (Actual) dill 1.67E+03 V, Velocity of Stack Gas fpm 8.72E+02 Curies Radionuclides per sample pCi 0.6 • Crad Concentration of Radionuclides pCildscf 0.0023 ERrad Emission Rate of Radionuclides pCilhr 1.859E+02 • Values below the detection limit are not included. M5 Nomenclature %1 = percent isokinetic, percent A, = stack cross-sectional area (ftl) ASI'IP = see "I'IP Btu = unit heat value (British thennal unit) Bw, = fraction of water in stack gas Co = concentration of particulate matter, back half (gr/dscf,lb/dscf, etc.) Cr= concentration of particulate matter, front half (gr/dscf,lb/dscf, etc.) C""", = concentration of metals (ppm, ,Iglftl, etc.) atomic symbol replaces "metal" CO, = percent carbon dioxide in the stack gas Cp = pitot tube coefficient (0.84) C -species symbol replaces x . x (avg)- Cx (oorr) = actual gas concentration corrected to required percent 0 , I'IH = orifice pressure drop (inches H,O) I'IH@ = orifice pressure (inches H,O) I'IP = D = , stack flow pressure differential (inches H,O) diameter of the stack (feet) D" = nozzle diameter (inches) EA = percent excess air ER" = emiss ion rate of back half particulate (lb/hr) ERF = emission rate of front half particulate (lb/hr) E RmmBtu = emission rate per mmBtu or ton of fuel etc. ERx = emission rate of compound which replaces x k-fact = multiplier of test point I'IP to determine test point I'IH L = length of rectangular stack (inches) mBtu = thousand Btu Md = molecular weight of stack gas, dry basis (lb/lb-mol) MF = mass of particulate on filter (mg) MFP = mass of particulate matter on filter and probe (mg) mmBtu = million Btu Mp = mass of particulate matter in probe (mg) M, = molecular weight of stack gas, wet basis (glgmol) N, = percent nitrogen in the stack gas 0 , = percent oxygen in the stack gas VI'IP = average of the square roots of I'IP (may also be referred to as ASI'IP) Pb", = absolute barometric pressure at the dry gas meter (inches Hg) Pb, = absolute barometric pressure at the sample location (inches Hg) PG = stack static pressure (inches H,O) P, = absolute stack pressure (inches Hg) PSld = absolute pressure at standard conditions (29.92 inches Hg.) e = time of test (minutes) Q, = stack gas volumetric flow rate (acfm) Q, = stack gas volumetric flow rate (dscfm) Qw = wet stack gas std. volumetric flow (ftl/min, wscfm) T, = stack temperature (F) T Sld = absolute temperature at standard conditions (528 °R) Tt = see8 M5 Nomenclature um ~ mean molecular speed (cmls) Vm ~ sample volume (fe) at meter conditions Vm"d ~ volume standard (dsc!), sample volume adjusted to 68°F and 29.92 inches Hg. V, ~ velocity of stack gas (fpm) V we ~ volume water vapor (sc!) at 68°F and 29.92 inches Hg. W ~ Width of rectangular stack (inches) Wtwe ~ weight of the condensed water collected (grams) Xd ~ fraction of dry gas Y ~ meter calibration Y-factor (dimensionless) Method 5 %1 = Vm d ' (T + 460) • 1039 I (8 • V • P • Xd • D ') 51 S S S II A, = (Ds' 14) • Jt Bw, = V wi (Vm"d +V w) C" = MB ' 0.01543 I Vm"d Cr = Mrp' 0.01543 I Vm"d Cx (,orr) = Cx ("g) • (20.9 -desired %0 ,) I (20.9 -actual %0 ,) D,q = 2 • L • W I (L + W) D"d" = ;/{0.0269· (Pbm + 0.0735) I [(Tm + 460)' Cp ' Xd ' ;/[(T, + 460)' M,) I (P,' "'P))) EA = (%0, -0.5 %CO) I [0.264 %N, -(%0, - 0.5 %CO)] ERB = CB • Q, • 0.00857 ER " = Cr' Q, • 0.00857 ER"",,"to = ERx I (mmBtu I hr) K-fact = 846.72' Dn4 • "'H@.C."X/' Md' p,' (Tm + 460) I [M,' (T, + 460)' (Pbm + "'H 1 13.6)] Md = CO, • 0.44 + 0 , • 0.32 + N, ·0.28 M, = (Md' Xd) + (18' Bw,) P,= Pbp+(PGI 13.6) Qa = Vs • As Q, = Qa' Xd • Ps' T"d I [(Ts + 460) • P"d] Qw = Q,/Xd Vm"" = Vm • y. T"d • (Pbm + "'H I 13.6) I [P",,' (Tm + 460)] V, = 85.49' 60 • Cp' ;/",p. ;/ [(T, + 460) I (P,' M,)] Vw, = WIw,' 0.04715 Xd =I-Bw, APPENDIXB North Yellow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data Yellow Cake Dryer Baghouse Preliminary Velocity Traverse and Samp ling Point Location Data Particulate Field Data Grizzly Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data B North Yellow Cake Dryer Scrubber Prelim 8 pts blank facility Denison Mines Stack Identification North Yellow Cake Scrubber Date / Z 4-I-:J-II!) r Barometric Pressul'e Pbm Z'i·~ in Hg Pbp Z. «-S J. in Hg N '0 Static Pressure (Po) -0 ·O VSln H2O Estimated Moisture (Bws) , 'Z.-' % Sample Height from Ground -:}-u feet A Comments: Stack Diu. 18 RCr('.rl!flCC: 0 POrls <Ire 9.5' Upstream from next dislurb::mcc Ports nre 9.5' DOWTlslre::ml from last dislUrbance Traverse Percent Dista nce From: Ports Point Diameter ID Reference A B C D E F I 3.2 0.58 0.58 2 10.5 1.89 1.89 ·b~O .0 <d- 3 19.4 3.49 3.49 4 32.3 5.81 5.81 • O&-~-. oS' I 5 67.7 12.19 12.19 6 80.6 14.51 14.5 1 . OS'~ .0,3 7 89.5 16.11 16.11 8 96.8 17.42 17.42 . ~ t(if' ·OS-I> Averages: Ts __ _ L Flow ---II P __ _ ..JIIP __ _ KEY :> liP L flow l ).. , '" '- .x _____ Fii!ld D:ua Sheet FII", ;~ 'rVETCO IL. ~ ..... ~ :t-y Sample Be.\( --'/ ,,- 1'" "" Z-- Plant Denison Mjnes • location' Nort Yellowcake Dlyer Scrubber Operalor'_-'-_t D", / z./ f/,Co Tln,;:"e Time DGM .p "., Clock Min (6) ." , .. up: Stack (T.) In = 1 1:5 o 1\ ~oH"I'1II,o-<5'1I . Ii 1-1 ·(,'tll '~II/OS-I t.ltS1 tclY'1 "/-"t 11 t.{.<;;1[l;Y1l9-1 .!. ~ ~ _3 _3 4 60 114 ;f.."l,YII·o(,<,II/·(»)II:c-OSIlCfIII(O I-u.o 1'2.&'{I1..f61 <::'7 11 <;;:$/1 fo"! 75 11?:-t(p ·'i'l/I.nl·wlll :~ I·$;:' IISII \\0 I tt;(.,It.'fl1t."P I ~\:i Ilq-z...1 (l3\. 90 II '6;-S-.~." 0 I~I . '6 Z-I -$"Z1~II1\t.. I HOi 'Z-1R1}z, 1<')1 5''6 L"1'1 U c:? 4 105 11'6~'\·1-1i')ll ·ot,"1.>II .,,'L 1·~v ll5' II [II 12t.'l-1 tl9''\1.,,,101 <;~II ~!oI ICf1 5 120 11c..1.,·:t4~I D<;1I.Ct') I .Ct'}11 (P II IlD i1.,t. \ 11 '\-')1'1111 1 {pvll q(JlllD ,,. __ 5 135 II 2;;n~11 ,O,~ ,"t ., 1·"1'" IrTlll~1.C;'f1 i1-11t.~0'll1 '1'<1 1 IIV. 30 __ 6 ~ S-6 -- J 7 '5-__ 7 ,0 8 4~ 8 '-f Tolli Averag1: 111,',<;'< 150 II <;,<1(.&1 D,llo7~L5--(" I· ~" 1111r-lcDLt:~W1 v\Q-'11.\..~'d II I Qb~7 165 II q \) \. ~V:\II . () <;-111 ~'6 '7 I . Y? II '6 II II \ I ;2.:X~1 '2. L!5T 1~ <{'''\j C)(II tw I /11 " 180 195 210 ~II ~~~1~' T3 1··1~F~rILOl1)&p'~3fZ11.1 (Pi 11 051 liD \ u... '\..4,~·i·1, -1._ " PaS\! _'I_Of-J, Run #-L i 80 N A Port Rcf.:rcnce _00"_ 9.5' 9.5' Upstrclm from ne.ltt disturbance D('I\',Tlstreo.m from IJSl disturbance Assumed Moisture 4-13 % PlOb, 2,1,1:> CP-2J..i Nozzle Caltbralton ( .)&-'L-,~~I ,~ Avg On . -; ~ J mches G"B,£ f+c..-I Console (, Y.F,"" 1. 0) l) 'H~ L.21::i" H,O Barumctr1c Pressures :)$-0 Pb", z,,-1. ,C,D in Ilg Pb" z....w{ ~ ~ in Ilg Po -04.<;;-InH~O f!£ J:Qg () '00 <{ () 'DO 'Z- LI=~\;Ch~k f,'fr:un .... ;: III HS Z1::. 1$ PIleI R)~~ LJ· 0 "H,O~> W31er Collected g Timt! Sampled mm Review K-@T", K-@To:> ! i1-<.k A-C\-..-L~,\i J.-.f\<-I/f>-L. Cllmmml1. '(, T' -'-I,C4-V 0 ~~ \ \. " l>cI ~ (1) r> l,.. J.,.rf c.. ~ '1.",.,..J F i \ '\-.... ") b .... h ~\L vW ,,~v . \ ,j .... / L;~: :v0~ D \, vA \ U ' ,v ;r... 0~ .e-t ? ~ c. l,""" G-.\,,-J (2v _____ FldJ Data $h(o:t q.0ETCO fZ fIlter 5M . Sample BOX_J,.L ..\ Ii ~o ~>' <) '> J" .. s- (p is ,0 -..- t ( ,- '" " s- V PI:snt Denison Mine, ' D,<e' \ t, :vI \" , Tfl~:-;t TIme DG)'l AP j,H :r HoC) V~,uum P"'''' Clock Min (9) \~'J \;"":0) De~ired Actual (.oil'; 1 ,«:,,~ 240 l'ic". bOO '05")-.')y ,'i y 'V 1 255 <3i-.05'.1 1·0t7t> ¥"1 .~ '1 rv 2 270 <t~. "ll·n -.0110 '01 /. <> "l 2 285 N ' (P ts 'V$~ .c'1 (·0'-1 1;;1 3 300 I <if"-.S' ~'6' .r:;k'Z .!( 1/'1/ It! 3 315 "1 1:>.'7«"1 iP4"'t<' 111'0 · I I . ovl '-,- 4 330 lob . t.{ np llilC> 1·0;'-J 'O ~ fo 4 345 IIfn . '2...T& 'O'i' J·o'1 1-<,.<1 5 360 111 ... !tdo'i V""" If·tt I· \ I , 5 375 j)(P .D'("l .051 ,,,>t,-. c,(j 6 390 HS ."(~() ·D5 ''1 I ·41 C- 6 405 1 ~, ·1l01 'OSO I'id ..... v • 7 420 }h~ .z....e> 00 .", ''1 -:s I 7 435 (1: 7. (" "\.\ 'oro .S-,/, .,0'" tU 8 450 1'O t... .1-&> ,&5'0 .~'6 ,y>-rJ!. 8 465 1<1 \.qc,.t-'O~'1 ,~ ;. . y 'l [1> 171.0', 480 -z...C;O. <;,,_ "1 I ,>2. Sf !. '1 ';:(t-<~ • .:. 14'\· '6"1'0 TOlal d. Zfl1'.1t,.~,\,<l.b~') 'It ~'7\) I , {'1\'1 C'\l~ ~~ Co,",,,,,er.t; location: North c!lowcakc Dryer Scrubber Operalor:_-+.b"'\ _______ _ T.:mp;::rJ.lur;::s ("fJ DGM Temp (T"I Stack (T,) Proix:: \ Fiho;:r '''''''' Efflu<:nt 0" '0 l("l/ I 1,"1..-1,.;D 1,'>0 ~ c, '1"1 \ I 'S 11M/-\' 1 o.l )( '1'1-. I, 1/ t; 101t7 '1[ -z, 1-7 1"\ 14-,7<" 11.";:;-1: I~ '> '1 /;\"(. il; ;-71~-" 7-~ °1-5"1 I. If ''j() JoO \ l \ ,1'(;' 'I.'{ H (;5 <t ¥ '10 f)"', ?1-0 1/1' &v I", 'd-V> '1"1 I'll.{ 1-1.' ~'" 1.(,"1 fnll7 '6' '1 ?f' 'h'" 1.~ 1.U l~~ IU '{ '1'1 o"l 11.'-1.K "lSt I,;' '{:j 10;' W( '/.. ~ -z" Y.J-(off IQo t alP . /O .. 7/' 0 ,,0 11:1,,) 11<0 111..-to ~1 In[ 1-U-V~\ ' t--' F7S "'It-tv "" / t )(p '1-'3: '2.">\ 1.1{.' 5S-"'I ( ~D " II~' 1.' t.5'-t 'v'5 ,,\0 ~\ 1 D't vb~ .{.. 1%1, 'lU r;'-r ~\ II!? !" I()~ 2-l.<" u., S'{ '1\ ( () !" - - h~7 (A "\ \\\) q~.-\ Page.1.--oC ~ Run # \ i "0 N A Stack Diameter 1 S" Port Reference _0.0" Pons are 9.5' Upstream from ncst dlsturhance Ports are 9.S· Downstream from laSI disturbance Assumoo MOisture 4·13 % P,ob, 'l-., .lP Cr~ NO?;l' Ylibration -:> . q .,.,'2-.~'1 1-. '7'7 Avg D".~ i:;:---- Gas Bag ~(..-\ Console -----.it Y.FaclOr \. <>t ~ AH@ \ -51' ';" H,D Barom~tric Prrssurcs Pb", 1,,'"1."10 0 Pb, 1... '"'\'7_!> P,. __ -....::·O:... .... ~S in Jig in! !g in 11:0 L.~lk Ch~ck Pre ft'rmlll D ~()~ PUS! 0-:0 o S- ~'1!\HG 'Ll-1'7 D.G =u P,IOl RJrc ~. 0 Iofl:O ·'22 WalerColiecTed ~ min Time Sampled ~\ Review K'"' :@T", K -@T", ____ Field Data. Sheet ~ (.l.{) TETeO A Filler __ "'_ -S!lmple Bo". V (I" '1 Page ~ of 'Z..-Run;; -Z- .:b-I, J' ... , .2.- I~ )' .. ( -'i Plant Denison .zx:~ DaI" \ 'f I ~\) LUC3lion: North Yc ""cake Dryer Scrubber Operator: ___ -'--'-i B-G. T~d POint 1 1 2 2 3 3 4 4 5 5 6 6 7 7 8 8 Total Average Time Clock Min (9 '/ : ~L 0 15 3D 45 60 75 90 105 120 135 150 165 180 195 210 225 240 N 6P aH (~.">OJ II V~cullm II Te~peralures ;fl IXiM T~mp (To.) DaM (~) (;"KO) II D.::sired I ACtual II ~Ifaj II Slack(T.) I Probe I P,obcOut I Filler I Effiuentll OUI 1o 101 ·5"D-1, 11650 11 -~~lllo'l 1z,,:,oIt-I¥1/ I ZGS I {VIIs'd1 s-r , A Ii c. 10 "!I AI ."" J -V Lo"f '1.V1 u,5'" Ut. '117 -tir--'}-V S",kU"met" 18'_ PonR,r","" _0,0'_ l \ ..,( .00; . '" \ -'\ \ "':> 1':>'\ 1,~ 1:2-11" '1.& « ---'i 3 L1.lt. ~ u Pons aI' 9.5' Up",,,m f<am ",x, d,,,,,ba,,,, IzY·llv-·o /·<>5 I· <>5 ~ ID,~ I v,'J "L-f'V l/j-r; L.I,) -fO y> Poru,,, 9,5' Dow",'",mr,oml,,,d,,,,,b,,,, 1-;1-.y-z.,V '0'5 .~, . "i ;, I'll q "1 N~ ~,,{g ,,'5'--J t/C(' 1-3 '6"'1 Assumed Moj~lure 4-13 % 'c11 ·0lP II·osVll . 'II I· '\ I II '1 I ~ 10" h. ",~-11.lt(' L_t.«~ I L-! '111 ~51 OJ I I~·}t-n '0)'0 11 Ao !.q,0JL'1nLLt>.1"_!1.-%-I1Yt"L'Z-'{i-1 7-1I1 di/T~T /~U'70 II·o>o~ .q() I·'" oIL '5'.11)0"1 !"/..;~ !1A'l I '1.,'\~1 ~\ II r 1'1 ~-v 11-'-I"'I1-s-1I 0'f'-'1I .C1"t -:-'1'7 11 s ll 10'( I'L)~\ "' .. (.(1.~---I~q 13"'~---r1--91-"l/ 1~.ni)ll ·o5"t.-i ."1) I .c,-t, 11';-111 00]---12-'51.> fi<g'" I-z.<-{.s-I s--J II yU I "y(p [0<{.<{oQoS'5'i -"\-V !''ll' II ~!1710 !'1-501 U1) rz:SIIs-l? Ilv> 1"1~ u-z.·ti--¥111 '0l-<;11·rr.ll'(G II 111(1./ 1-z..&G !Ub !i.$~r ",~ll9'S"I lo! '1,15.ooV I~I /·(-z,Ii ·(~ n~ )to 1'Z;~!'I1.(I>rz::t;'1 S>'1> II ~"R lOY 171/>·O~D II ''0(,0111 ·01-1,·61-11 1'JI 1(0 I VJ'VI'z:01 ~'7'11 '71' 11 <;;'1 I 101-1t-1,t.·'?WlIQ&oll, .• ti l. b "fIIT!1 UD. 1i1S'1'U.l(p I '1A(~ I 9'1. II t:\ \ I .Jot;. tl\-t·W II bW III'.unrV7'!1 lO ll I\V 1 1.-1-'>I1-~lU1-llPVlI <iii I ut '1.,.3 . t.f t. '>1 \ S-1.c-..-tO -I -I PlObo 'l t -0 CP~ Nozzle Calibration .~ . '3<' ~ • 3'i -t. . ~c, -; Avg Or. • 3J""Z inches 0" B.g t--lG. I Console r, Y·F~'O! l.u-t '>- dH. /.,,-}I '" H,O BaromeuiM P .. rcssurci Pb. z.+~' Pb p L -( ... ~inHg Po -0-Oo::;;{{ inBg mH~O Lelk Check p" O-:(;l>c( Po!'! Q.ber--ffl/mlO , .... mHg 'l..'Z--bQ P,tOl R!l~e O· C> [IIH'O~ D.D ~ Water Collected g Time Sampled 7l:1 min Review K- K= @T", @T. Additional (Extra) Leak Check 'nfonnalion DGM before Leak Check Vac ("Hg) Rate (fe/min) DGM After Leak Check Vac ("Hg) Rate (fe/min) --- _____ Field 0313. Sheet Fil!er=5i41E~;~le BoxL S-i ~V Pbnl Denison Mines, Location Nor! Yellowcake Oryer Scrubber Operator" -f--=-'\-D'~ (Z-ld' () Tr3v~rse J G;! '7' ''" __ 1 ." __ 2 -f" __ 2 >_3 7. \ \!, .. ~%"-_3 J .,, __ 4 'c'i" 4 ~ 5 I)""~ " __ 6 ~r 6 1--7 . Time OCH .. -! .P Clock Min (9) :,~> II ( .. lIp> I DC:51TCd [n Ut-_o 240 11'-7'1_S00 II~II-H 1-16' fll1.:=l1 n!q I t/'"\512.-5D 1i>115""1 II C;vl "I<{ 255 270 285 300 11 1..-"1t--l!i~'1II~SII I -()<P [-Oo-I! q nrSl1-tIT2.fnUliI 'it-II ")/1 lD 315 11'70~ -30"1 11~7JI-~ -:r I-'11 lm l l \~ I ZW I ~~ I Z $°1 s"<.{ II t1~ I /01 ~ I·a li (.~ m Ii 1. \ t~ 1.-' i) '51[ C1 \\-0 330 345 II i,il -fD1-FI1D$' \ Pi ') I -"13>11 A9' I! \( 7 I 2.'c\'1 1 H II 'Z1-'lf ceo I! q~' III ? 360 II-i, 5\ -IV') () 11 -f)S' II ,0[ I I -Cot III "'1--"IIU IT'-I I "'0--\'-\ 11 ... 1-Vj 1,151 1P-<;>-r C{Yfl\ '-1 ~1 '2,~~-~lo-{'{ll ~rl-~t ~ -i-JI tD11~~1."dl1.~~ ~11..!i~J ~10 3901, --O'P -q( -G\ fi /b"\ _ 1,.A. ~ \ ofJO/1 In. 405 r,,<;'l'flO?ll;o'Jl)11 -"In '" Ilrqil 10'6 1 fZ77t V>r -z,\tr.1 b I IIT6'1 1 In- 420 ,r --'--I 435 450 465 ;. __ 8 ~.-8 Y TOlal Average /t,:o;,-480 II L{ OlP -1" ( 5z..1-5"> 1',,.;+1,,\."·111$'1 '1~~ i St.. ..., v ,)01,\1") ,-:.1-.400 , .\<1 U'"' t.,.."') \ , ' l \00 '? -"\10,,\ ./ C~:r"'l'.",,1) f..: v'W" .. J,r-J." ,,\ \-v) At-?,,\--c.~ 4'1 S.x.. ,?'" () 't' I <:>"" \v w()\s'- <"1 t _0 Page..1L-or"Z-Run .ll:_L- i N B Q A Pon R~ference _OO~ 9.5" Upstre3m from nc:xt dlSlUrnllnce Downstre:un from last disturbance 9,5' Assumed Moisture 4-13 0;' Probe z. t -G. Cp~ Nozzle-CahbratlOn - -3">1 '?~~ -:>n_ -J"~:5 A\'gD~ " :> 9L.lnches Gas Bag -;:rc-I Consoli: z;-- y -FlIclOr I " (.)( Q "H~ I-S)! I "H,o B:;Irometnc Pressures Pb" Z 'f. ~ S=-;ftHs Pb~ Z. 'i" So-V--In Hg P" c). OYS In H:O Leak Ch~;:k Pre ft"moo 0 -6 V '; --.- \>:;;,nH,; 1. t ~ Pmx RJ:o O· 0 Ir.II~O .'Z.~ :...::..., IU fgg 0 -0 b &, IL 0° --z-i:{ Waw Collected (p 5" ~ "I !: Time Sampled »0 mlr. 11--" RC:\'le\\' K-,-@T", @T", Yellow Cake Dryer Baghouse Prelim 6 pis blank Facil ity Denison Mi nes Stack Identification North Yellow Cake Drve r Baf2hotlsc Date r Barometric Press ure B Pbm in Hg Pbll in Hg N 0 Static Pressure (PG) in H2O A Estimated Moisture (Bw.\) I % Sample Height from Ground fecI Cormllcnts: SI'IC,k Om, 16 Rdercm:c 0 Ports are 57" Upstream from ncr.\ distmhanc\' Ports arc 468" Downslream Irom last dis(u{b .. 111CC Traverse Percent Distance From: Ports Point Dia meter III Reference A B C D E F I 4.4 0.70 0.70 2 14.6 2.34 2.34 3 29.6 4.74 4.74 4 70.4 11.26 11.26 5 85.4 13.66 13.66 6 95.6 15.30 15.30 i\ vcrages: Ts ___ _ L Flow --- LlP ___ _ ~LlP __ _ KEY ~> ITs LIP ____ Field Inta Shect Plant· Denison Mincs DOl'. 12. ( 'Of t<J '·rJ.ycrsc TlnlC "",", Clock Min (9) 1 o~:;" 0 2 10 3 '0 4 30 5 40 5 5':> 1 to ::l~ .0 2 70 3 ,"0 4 "10 5 1,0 6 ,.0 I i\:;~ I ZoO Total " .... ·' .. 10 .. ("OI"mM:S. Time ~'.J< let: 11, .o','n I' :." TETCO filtcr 5" If"c Sample Box~ DGM oP 6H r-...,o: V~~m ta') ' .. liP) Desired Actual ( .. II" 'O«,,'~ " ' ''\ .' (., , '''' :> 8)3.0'S-d<{ ."~ .1>9 2. 838.'3;S' • Ie.; '''''1 • "'I "2- 8'i" . -;2., ·?I l.Q,l l.o t> Z. as/)· 'f?,{ -'1.0 """ [,.., 'L 8$1.125 ,to 1.00 I,OC 3 '0"4. S I'l,. , z.z.. l'o'\ I.e,=!: ~\ ~'''Z\.~~o .2.3 I •• 'S" i.'i' '\ 678.4'1.0 ,z. ;, 1.1 , \.(5" 5 'BBS. )'1'! "'I 1.00 l.20 '1 '097.51., , '/,0 \,00 I."" 'i "~~.41.' '1'1 .95 .'11' <I ~o". 152. 1"j.2.o~,r , 5.11~"'I./ ~3 / .0.{ 3'11 91."\ Baghouse t1P Time Baghouse 6P '·1 W2'S' '1..0 /. S '.u I.' Location: North Yellowcake Dryer Baghousc Operator: M,M~~WCc: Tcmpcralurc~ (Ii St3ck cr,) Probe 7) l.'/. ., ,f 1.~O '6' 17 " I) Z30f lI-Z" .. 1'1 1)6 "7'7 2.~" 77 2.70 78 Z.,g 76 2<., 19 U~ 7~ z..5\o 3.2:,'D J 'l u,l Pr:llxOut Fiher Efilucnl 1.40 2.7'3 "1"1 ,(,z 2."5 "tb zi9 2:JO l{~ l{',! ~70 ql 7 f, a..\o 't'! l1~ bo So H> 'l7e -'i~ 2'4 2.~1o '-I'{ 2f.,[ t.6<J '1'\ 2."9 2.r(" '1Cf '/.~S 2~t 5( L..?3 Zbf Sl. 9 Do..'fe-15 nGM Temp (T .. ) 0" i, r.r ~'i "8 b\> 71 bS ,4 10 h7 7'- 7'\ 7'f '/'1 lp 8<: Tl 'de; 7€l t;r &:l 97 ez.. 89 9" ! '0') () / If.,:3 ~V'''''' Page _I _o, __ 1_ Run #_1_ i B AO N SlaCK Diameter _16H __ Pon Reference _O.OH_ Ports arc Pons .:Irc ~ UI'5trcam from nest disturbance 468'" Downstr.::am from Ia..~[ disturbance Assumed Moisture --~_% Probe ~ Cp~ Nozzle Calibf3110n 1-z.. .... U:> Iz'''''' Ill) ~2.'7(. A. ... g D" It..." I, inchcs Gas Bag Ambient Air Consolc _'1-'-__ Y.fac\or \.oo"t.. :.\Hc l· 5 11..{ in 11:0 [laromctr;c Pr.:ssurcs Pb... "2. '-1" <.5 in Hg Pb" "1o.(,.>e inHg P(j -. .1.1 inHtO Leak ("~~k IN ft'fmrn 1:2.00S' ........ ·",II!( 2v·O P'IOI.\Utc 0 .0 In H,O ~ Watcr Collected Time Sampled Rc\'jcw fog 6.ooz.. 1.0 __ 2..: • ..0 ~ 10 . "\ 1.1:> ~ K- K " @T", '9T, =.".. , min Grizzly Baghouse Prelim 12 pts blank Facility Denison Mines Stack Identification Grizzly Baghollse Date i Bn romct d ePressli rc Ph", Z--t.S-U in I-Ig Pb, 2.-(;/. r.J'in fI g N AO" Static Pressure (Pc)-' DIR. () in H2O Estimated Moisture (Bws) I % Sample Height from Ground S e:. feet Comments: Sl:"lCk Oia. 18.75 Reference: 3.0 Must use 36" ~robe or lonser to keep box outside handrail Ports are 24.5" Upstream from next disturhance Ports lIrc 48" Downstream from last disturbance Traverse Percent Distance From: Ports })oint Diameter lD Reference A B C D E F I 2.1 0.50 3.50 2 6.7 1.26 4.26 b or <tS'"" w '0 3 I 1.8 2.21 5.21 4 17.7 3.32 6.32 f> .I)"r I·~ -f:Q,{o 5 25.0 4.69 7.69 6 35.6 6.68 9.68 ~r . 00'..--,~ o~-,- 7 64.4 12.08 15.08 8 75.0 14 .06 17.06 {py ·ols ~'l--o'o 9 82.3 15.43 18,43 10 88.2 16.54 19.54 t.V • cJ G a b/;;;-> - II 93.2 17.48 20,48 12 97.9 18.25 2 1.25 Averages: Ts ___ _ L Flow --- 61' __ _ ~6p ___ _ KEY => /' . S Field D:lI~ Shetl PI:lI'11: D.:.n~S~Minf!tS "". IO~{q / ,0 I ,i (' Tr::;....::,$~ II Time 1>",'''1 Cloc~ ! Min {il) DGM "'I TETCO d Fdi:-r ~[,rL 53mple 8u:.:,~ Location. Grizzly Baghollse O!k~lta! Pl DGM Temp ,"r .. J ,p I '"""m i--,----'-:::r==.::.r- ' .• HO '"' .. ~) SI3c1..:{T,} Fltler I Ei:lu:t,dl QUI I fn p .. ge _! _"r---+, ~un;!.---1 i N AQe 2 ",-, '-;r'6 & • 13-;, . eSC -"17 . <; S 'V (" '1 1.. 3 0 z.,cW z. <.{ () S-~ iJl (P'1 s",' Di"n,'" 18,75' ~~t5 0 'f1~.5o-", ·D';'o ·sl ~~! £.... _(~1--7"\ 'l...-f'Vz.rc lul. !(G " {;n Port Reference ~ I f¥v"-3 4U 1-"1t. &(,,<:: '~5'6 ."1 (, .'i t. 1--:rU 1A'I. 1,.'H t..,~ 1<;,,1-it f (., Po""" 2'.5" Cp"'"mf"m"",dI,wI"'" 4 [,0 I ffJU. t1<t'-1 ,o_55 /·0& ~(Jfo -z.. f-J ~t.{-t., '2.:~ =:0:1 <-"X-r1 1-~ Por<sare 43" Downs:reamfrom lastdiSfUrbance .... 5 .. <> <;-z.3.<{0' ,,05', \'O\' !'blJ V '-U i'ZC;v/ 7)-/Z, ~}:rIe;"1 «I Be "Q~ ,100 11»1'ln\(' ,o ~o ).11. H(O 1.; ''V '1.,!-0 1-",4 z.,,~ :$Y~. y<';- ... 1.., ~ ,,<0 Lq,G'! ~..jc", 0S'5 l'oC, Hl "J ~ vt, 1. Vfi 1A 7. "7< ~ 51 g-"'j ,0 8 ,'(0 ''?(P'l .~t.(p 'ChI) .~o) (·'Z.v &1 1''1 ?'{'1 -Z-~ "2"')< ~& f '5' "V:) '"'~ 1 ~ V Ij'f-'l. ;; t -075 ! ./l.> /. () "1/ 1---l-1:; C 1'Z.. 1-30 C.: q '1 J" } hI'S 10 \Y"O Cr'''It,.'l,<';'1, -o"\C -'60 ·\:O --UI 1(,; YiD 1--\~ 2,'tu ~-'L I, c, t ~o 11 2.,0 0"C '1WDbl 1-1.,1/ 1,-'" v ' £'sO 1f;( '-LI' 2l\\ <;-i 1, qll "0=B2 ' z.lD "1lq·7I\·!-" ·o( )·10 ·lU 1.--(;;1---z,<..j 1 1~~5 1~\I ,<:0.;-'1<; ,f.,? ,,4,,> 1 ~ NC>I~»).lGJ", ·r)'; l·lV I'[D V 4r/ 11_<:' '?~11.q'-i t.J q <f i •• 2 ''7..~() c, .. q ... "'Jt" -o5'f,II·lv l'(O !..r 'if/{ lih'V1>..f U 1..<;0 & :t .. "U ~.~ tYO "1(.D·{':n ·OiP(' /,[1( Hq l/ '()" 11."f?7,7'1 -V 7 s-I 'l! (57 ,-h'f ~ 11, ,,0 -"l.' -I .~ i\ ·OK 'l·it) /'( p I 'v s((!) V-IU 7.'C Z...-t;i: I q-<f 'if'V ,0 5 ."t.0 t1&: .'1c{"1 -05V . ." . lie, , V x.:-t )-5".2 1,-'1-5 1"Sc 55 tt'-f 40 6 .,..{o "1'1 .'}0'6 ·05 .\1) f.ID -V G -1' .0. .... U,C; L.(; Sb 'd-"i 0 Ii ~-5 7~l?O /On·(,)! 'n)" ·\0 1,1,0 'V '--r Z.~) 2/,'..,. 'V" I;-·t ~ s:-'1 ." 8 <.(/0 jDZIP.5o<...-·en ./ () 'f· (j'/ ~ '? 7.~ I?e-C-!?S_<<< '5-~ '6~ JtJ 9 '1jO ID'ID,<1H .()hb 11,lv I·IS "7 'f'" i/'l' 17_ 1,-t..<;( bY' "1 f) "11 ~ ~-J 10 ..;<V IOS{.UWr _0$0 .'1"1 ."1'1'< '6'1 1.7' ')jiS t..1t III S-~ '1l ~v 11 <1,,0 IO~'\.'5'tS' 'O~u 'Q"1 .c,'i ", '6 'V{ '''10,+ -LII ilLI"1C fin .(0 12 , 4~O /O~'J.';u-1 '0«') dr'! ·ctc., '// oj} 1.,-1 '2J<'1 ~">0 (;b I Cj D ct1 --,~ ~ I D~:1:0 ' I TOlal ;Z,J,bl t...,J ~?.., 1--'5.z..~ - .,.;ofI.Y -- AI'''',. .1."5 1 \ 7' Vi 1') i4 \ .0) -( l Vj u-z.- 1'1· :, ---t.{ I (P [ ---- ~(.,.l- ('om:m~IS \ ~"'" '\-I --- ...;.4\ {\;'. vi. '{ .1' '0 ~ ? ( b7 \-pc> -.Jf Il '}{-Q'oJ 1'~ 1.-~ <1\ " ",. If VJ ~ w-"'-<' {.J, 1-. ~" IA~ i.()b '7 \A'Y " Assumed MOI~ture % Probe .l&C ~/ CP~ Nozzle Calibmuon .~ ~ .Tl}-.nJ.- A~'g Do ' ]. 1-& f inches --- Gas Bag Ambient Air Consok '3 Y-Facto; (-0 Q ~ ~H~ L..fe.J!i.<n H,O 3arcmelnc ?ressurcs ?b", 2=1. -~Q In Hg ?br 2.. c.{. '-{ TmHg Pc, D· 0 t$-() in H:O v.zk o,~~~: Pre f:~/nl:" 0.005 "3~:nH£ 1..3. 0.0 tTl J Pl:oIRll~~ !n H:O~ ~1 " M" ( .~ LS:. (j.U .6"2..5""- W:lter Colkcted t 0 ? g Time Sam~led !1 4 ~o !TlIn n--r" 10'1 R~vlt:w K'" K- @T". @T", North Yellow Cake Scrubber Sample Recovery Gas Analysis Data (ORSA T) Yellow Cake Dryer Baghouse Sample Recovery Gas Analysis Data (Ambient) Grizzly Baghouse Sample Recovery Gas Analysis Data (Ambient) Chain of Custody Lab Analysis APPENDIXC c North Yellow Cake Dryer Scrubber METHODS Facility: Den ison Mine Date: ------- Slack Identification:..!-N:.:Y,-,C::.., ~Sc"-r",ub",b",,e~r ____________ _ IM'>'NGERS IMPINGERS Run: ( Sample Box: (13 Impmgel' Number 2 I 3 I 4 I 5 6 Initial Volume of hquid (H20) in impingcrs, (ml) drop out I 100 I 100 I Silica Gel Final (g) -=-=--'-'-'-i-':::-'----!--t:"'-i~:+__+__';;.::.....--''+~~'---t-''-'-'!.>....L I nitial (g) --'-;-7.iMH->L:s:r-:-t~r.,-'-:J'+--:::";::79--":c~~'l-Lf'T-7- Net (g) d'!!"~b!:=!!fl:;b;,.\4~';';;dd:=';;':;;"'d:d:.b~"b~";""=:b Total (g)========= Run: Sample Box: 2 IOlnger Number I 3 I 4 I -z-6 Initial Volumt.: ofllquiu (1120) in ililpingcrs, (ml) dro out 100 100 Silica Gel , _____ , ___ ______ ______ ____ _~~t~I (~=_===_=_=_-==,=== _____ .. _____ ____ _ ____ __ _ _ ____ _ ______ _ IMPINGERS IMPINGERS Run: Sample Box: 2 Imjlgcl' Number I 3 I 4 I 5 6 inilial Volume ofliquitl (HlO) in imp ingcrs, (ml) drop out I 100 I 100 I Silica Gel Fi nal (g)------t-----+---+---+---+---- Initial (g)------t-----+---+---+---+---- Net (0) ====~====d=====~===d=========== Run: Sample Box: Impinger Numher 2 3 I 4 I 5 6 Initial Volume of liquid (HlO) in unpingcrs, (1111) drop out I 100 I 100 I Silica Gel , Final (g)------t-----+---+---+---+---- Initial (g)------t-----+---+---+---+---- Net (g)===d=====-===='====='====,,==== Total (s) ========== 0<--'\, '.~ V"\.I-t l' Plant __ ~_ " OtZ-SQ+ Analytical Mcthod _____ _ Date IZ./-rff () Test No. r Ga$ Oag No, He.. -I Anob;enf TCnoP~ Operator Dule /',-k;. Q Tc.st No. ~ Gas (lag Nu.l_1 Aonb;Cllf Tenop ~ OpcrMor Dale ---TI.'SL No, ____ _ (;as Bag No ____ _ Alllbi!;1l1 Temp ____ _ OpCnlIOI' ____ _ Location, ___ .!..t1I,,_..lV-=C=-____ _ "" Nt:1 "" Gus --:',5 '?I ~f ~.r s . .> 1'1·1-1"1·1-I", . 't.. ·f Nfl No< N~I Gus ,,"1 ~.? "!,. J $.~ g·3 ?$ I q.-{ Ie-! I C. I "" Ntl NeT Gu.v tOl was determined using a gas ulIlllY7.cr CO is not ntCllsurcJ, as it has the same moleculAr weight as N2 AYcral;C Net 5' I'" . V Average Net Volull11: ~ . ..5 Ie, I Yellow Cake Dryer Baghouse Method 5 Dute: --,-f 'P'-/t..!:.lf-J-I_vo __ Facility: Dennison Mines Stal~k IdentiJication: North Yellow Cake Baghoust.: Method: 5 IMPI NGERS Run: Sample BClX: « Filter Number: _ <;;L (0 "1 C, 2 I 3 I 4 I 5 l mtgcr Number 6 Initial Volume ofhQllId (H20) in impingers, (ml) tOO 100 I I SG I Final ee) f;D() Initial (g) ttt 'S ~ J Net Is) ('i .. <.. lev~t l %~~? I~;~jl pII ~ Vic "" IMPINGERS Filter Number: Totol (,,)=:~I =O===j:l:::===== RfNSES-------H;O ······ Final ____ " FinaI ____ " Initial ____ " Initial ____ s ml Net g Net g+ 1.32 glml "- Run: Sample Box: 2 lm~)lnger Number 5 6 IlIltill] Volume ofliqlJ1d (H20) in implngcrs, (ml) 100 100 I I SG I Final le) ____ t-___ t-___ +-___ + ___ + ___ _ Initiallg) ____ I-___ +-___ -1-___ + ___ + ___ _ Net (e) __ =~= __ ,b __ d_=_4:===h=== Total (g).""",=:::::::::::::::::=,,,,=: RiNSEs·----· -.-.--. _. H,O .. ------.---.-.---.. ---_._---.-CH,Cl, Final g ---Final g --- pH ~ --Initial ____ g ln itial ____ g Vic = ml Net g Net g-+ I :nglml .. IMPINGERS Run : Sample Box: Filtt.:r Number: l mpingcr Number 2 InitIal Volume of liqUId (H20) in llnpingcrs, (ml) 100 100 I I SG I Final (g)----t----+----+----+---+---- Initial (g) ____ I-___ +-___ -1-___ + ___ + ___ _ Net Ig)===d===,:!,===,,±==="'====.b=== RINSES .. ____ . __ Total eg)== .. _;_; .. ;._;.;._;.; .. ;.;. ;.= __ . ____ ....... H,O CH,Cl, Fi11al ____ g Final ____ " pH ~ __ _ Initial ____ s lnitial ____ , Vic = ml Net g Net S .,.I J2r/ml ;o; ml ml nil Grizzly Baghouse MethodS Facili ty: Dennison mine Stack Identi fication: Grizzly Dale: _/..J/7:L..J/(:......c..tf_,/ (~tI_ Melhod: 5/202 IMPI NG ERS Run: Filter Number: Sample Box: lmiger Number 5 b<.\'-2 I 3 I 4 I 5 6 luitial Volume oflillU id (H2O) in illll)lngcrs, (ml) 100 100 100 I SG I , , . ('>'5''-1 i;»'-/'-r 1-1 c'" 1-/61A 1- 7ci., .1, ("13 . (p "ll{. I q 5"1-.'1 Final (g) Initial (g) Net(g) ( '/..,\.)) 'b\. \ s·'" 5:;>' pli ~ -- Vic= / Total (C)===~=o='=l!=:= H~6 -CH,CI, Final ____ g Final ____ g Initial ____ , Initial ____ g rnl Net g Net g -<-\ J2g!ml" IMPINC ERS Filter Numher: Run: Sample Box: Impmger Number 2 6 Initial Volumc of liqu id (1120 ) m impingcr.~, (ml) 100 100 I 100 I SO I Final (g)----t----t----t----+---+---- Initial (g)----I-----f----+----...I....---+---- Net (g)===d:===,,===:d=======,,==== Final ____ g Finnl ____ , pl-l =--- Vic = Initial ____ , IIlI Net Initial ____ , Net &+132g/ml" IMPINCERS f ilter NlIlIlber: Run; S,unp!c Box: 2 (mr nger Number I 3 I 4 I 5 (. Inillal Volume flfljquid (I-I}O) In lI11pLng~rs, (ml) lUO JOO I 100 I SG I Fin al (g)----f----t----t----+----+---- Initial (g)----f----I-----f----+----+---- Nel (')===d:==="===d===.!:===b=== TOlal (g)======== H,O -----'--cH,ci, --_. ' .. -... Final g Final g pli = ___ Initial g Initial g Vic = ml Net g Net H +1.]2 Rlml - Ill! ml .01 Chain of Custody Record TemperaturB on Receipt __ _ TestAmerica Drinking ~tsr? Yes 0 No 0 THE LEADER IN ENVIRONMENTAL TES"[ING , ...... -4, .... \'UU'1 Q:em Pro,", MsrUlQ¥ D.J:e Ch6i1l of CiJslad!t Number Tetco Dean Kitchen 12/10/2010 Addr~s.s:'--·' •. --------•.. --·,~OIH1Nlr.7bG,iA'Oo:!C()':JtJ)lFtJX/lJt.!m!:)cr LltbNI/,n/)er' 391 East 620 South 801-492-9106 Page Qf Gill' I State I,ZJ:I Cede --Site cai~ .. Lao C~JiY.1 Anafyt;Ls (Auach /istif American Fork t Ut . 1-$.4003 S~cttChnuon .. n)ly.nP.lm« , mora$paC9/sne&:!():;J) . Project NlJme v.d Locl!lion (S:a~l Ci4mer/WayDt'/ NiJrl,'.>Qr ! I: Denison Mine 2010 4th Quarter I SpeciallnstructJonsl COfltr.:l,;(/PlJrcfJa~ OrrJef/Quotc No. . GontJiners 8 0 i I Conditions of Receipt Ma"/)( P,"'eM;'ves ~ :;: Ie " I -(Con-t~::~~-,-.-:..,-e-/~~-,;,-~-~-::;,,~;e~sc::::,n<,>,",8""! Dale : rime ~ ! ~ ~ i l ~Il ~ ~ ~~ ~ ~ 3 ] ; I 5642 Rl Grizzly filter and beaker 10/19/10 i 9:30 X f "'\: X 1 . . . -r---;--+-+-+-t------- 5677 Rl NYC filters and beaker t.~; \\. ... , 12/7/10 j' 8:00 X! ~ /\ /.. KIX 5679 R2 NYC filters and beaker 1. \(: \ ~,. j 12/8/10 8:00 x i X' xi. ~ 5676 Baghouse Filter and beaker 12/8/10 9:30 X I P'-li ~ fA I 1 I! ! I ._-!! i t r ---+-+-+-'!~-r-r~4-4-+-+-r-~il -r4-4-T r -r-r-r------------- -----------t----t---+-+-t-H-t--t-t-· r-I . -t---~-'-r--:-+-H~-----, , I I i I I i ! i I: ! ! -.----_ .... ---_.-i I : i j -l Possible Hazard IdsnI;f:Clllion ISttmP~ u~w fA fcc tr1lJybc ~ if som;:J!e31JM r~~fned o Non-Hazelfi 0 Fl!rntM!:I!e 0 SKin Jrri/W 0 Poi:5::lf19 0 UnJm::llfm 0 Retum To Client 0 Cisp::;:safByLdb 0 An:tliwl FlY ___ A'h""Jthlt tonglNlIIsn 1 m:;nth) Tum Aroond Tkne R6<;uir~ QC Rcqllirc;mvJs (Specify) o 24 Hc<t1Yl U 48 .~fS 0 7 ~ys 0 74 ~ys 0 2~ ruy1; C otnor as Der method I. ReI""11BY ~./ ._..l~;~!_){,: jnm; ~ 1.~J~ay l[)ato IT(11ItJ 2. Rer".,,'i;:a-i/ 61< I "'''' I TIm< 2 Rga".. "" I "". I runo TR"'~.nIl~"'''Rv .......... .,., -.. ,", ___ " __ J"-. -.-------......... -n..-1 '-"""'" ['1<1'" !.,.n::::.A:/~CI""J'"'Y IV""",, Co:mn,nlS When Complete Email to:DeanorPaultetco@tetco-ut.com DlStRIBUTllijti;-W"rlItE-----:-R&lIJ~ I'; Cite", ",,11"1 Report CA."'ARY -StBys witn ~ SiI1'fJI9; FINK -F"~kI Copy FedEx " Order Fo rm , Ground Must be processed at a FedEx shipping counter. ,\ .' . , ,~ \ ", I( \,,1 -/.: v' ( I' ':\ \ (,I' .,';, . .',1,.. T ·' j -/. '/V i ., , 1 \. ,,.' , 1.. , .n.) Questions? Go to fedex.com or caU L800.GoFedEx 1.600.463.3339. TIl& Itdh GIOUM o,~" ''''''';, ,'" rid .. 6,,,,,1'4 '~"""nU "i\",,1II1 U.S. tv u,;.-; lIu. idb: G'ouod DIdo' fo< ... you ','" '" ~ II""'" ••• dill •• '." 1M bo<\ 01 \til S •• l .. ·• CGP1 01111:. ~'(II""'! ,.d in .hl <"'ft'" F.~E< So..!" G.v. .. ""I..:o.~ ,., .. , Itt" F .. " ... , I .1>'i<J. H.",~u. ",,:,.,1 ... ".,:1 b •• ~.j "~g.,;. fdt. G." .. "j Old" r ..... ! ! .~. ! 1 I l i I ! I 3 Puckagalnlolmfltion o Residen,i" Delivery Mdlen ~'iVOry Signature Options w",.".f,l<., .~ .... " ... " Du." ... ",J'''' 110 Sign.'ur. fltqu~ed. 0 Di.It' Sigllllull 0 'nJilfet SiaolMt '"h; •• tlboWl_Jlo!<",.. A'r<"~""~'-""'''' ........... , .. ""._ ... >!o .. , .' .... ".,"' ...... , ; ... r.:;~~ .. W',' :E::'{~~$~=~ 5 fedEK Homll Delivery· Premillm Servicll Upgrades R,,~""'I •• t. .... _ .. lOIlt<1.I .. ""·nr> •. 6 Payment Billl.: J r--("""lhA",~. "" ... ----, i!1l~~8~",~ 0 Rf<ipienl 0 Third Party [I Cr.diT C~rd 0 CI<h/Chetl ,." ....... Analytical Data Package Prepared For Denison Mines (USA) Corp. Denison Mine 2010 4th Quarter Radiochemical Analysis By TestAmerica 2800 G. W. Way, Richland Wa, 99354, (509)-3 75-3131. Assigned Laboratory Code: Data Package Contains 20 Pages Report No.: 45715 Results in this report relate only to the sample(s) analyzed. SOC No. Order No. Client Sample ID (List Order) Lot-Sa No. Work Order Report DB ID Batch No. -~ 42540 5642 R1 GRIZZLY FILTER JOL 160499·1 MCFPL1AA 9MCFPL 10 0355384 & BEAKE 5642 R1 GRIZZLY FILTER JOL 160499·1 MCFPL1AC 9MCFPL 10 0355385 & BEAKE 5676 BAG HOUSE FILTER JOL 160499·4 MCFRJ1AD 9MCFRJ10 0355382 & BEAKER 5676 BAGHOUSE FILTER JOL 160499·4 MCFRJ1AC 9MCFRJ10 0355383 & BEAKER 5676 BAGHoUSE FILTER JOL 160499-4 MCFRJ1AA 9MCFRJ10 0355384 & BEAKER 5676 BAG HOUSE FILTER JOL 160499·4 MCFRJ1AE 9MCFRJ10 0355385 & BEAKER 5677 ,5678 R1 NYC JOL 160499·2 MCFP51AD 9MCFP510 0355382 FILTERS & BEA 5677 ,5678 R1 NYC JOL 160499·2 MCFP51AC 9MCFP510 0355383 FILTERS & BEA 5677,5678 R1 NYC JOL 160499·2 MCFP51AA 9MCFP510 0355384 FILTERS & BEA 5677,5678 R1 NYC JOL160499·2 MCFP51AE 9MCFP510 0355385 FILTERS & BEA 5679 R2 NYC FILTERS & JOL 160499·3 MCFQ71AD 9MCFQ710 0355382 BEAKERS 5679 R2 NYC FILTERS & JOL 160499-3 MCFQ71AC 9MCFQ710 0355383 BEAKERS 5679 R2 NYC FILTERS & JOL160499·3 MCFQ71AA 9MCFQ710 0355384 BEAKERS 5679 R2 NYC FILTERS & JOL 160499·3 MCFQ71AE 9MCFQ710 0355385 BEAKERS TestAmerlca rptSTLHchTltlc vJ.73 TestAmerica Laborato ries, Inc. TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Certificate of Analysis February 4,2011 Denison Mines (USA) Corp 1050 17th Street, Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab Project Name Sample Type SDG Number I. Introduction December 15, 2010 Denison Mines 411> Qtr Blanding, Utah Four (4) Stack Filter Samples 42540 CASE NARRATIVE On December 15, 2010, four stack filter samples were received at TestAmerica's Richland laboratory for radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification numbers as desc ribed on the cover page of the Analytical Data Package report form. The samples were assigned to Lot Numbers JOLl60499. II. Sample Receipt The samples were received in good condition. The COC indicates sample 5677 RI NYC Filters and Beaker while the actual sample container says 5677 and 5678 RI NYC Fi lters and Beaker. The!D on the container is what was used. III. Analytical Results/Methodology The analytical results for thi s report are presented by laboratory sample !D. Each set of data includes sample identification information; analytical results and the appropriate associated statistical uncertainties. The analysis requested was: TestAmerica Laboratories, Inc. Alpha Spectroscopy Thorium-228, -230, -232 by method RL-ALP-OOI Uranium-234, -235, -238 by method RL-ALP-004 Gamma Spectroscopy Pb-210 by method RL-GA-OO I Alpha Scintillation Radium-226 by method RL-RA-OO I 2 Denison Mines (USA) Corp February 4, 2011 IV. Quality Control The analytical result for each analysis performed includes a minimum of one laboratory control sample (LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments" section. V. Comments Alpha Spectroscopy Thorium-228, 230, 232 The achieved MDA of the samples exceeds the detection limit. However, in most cases, the activity of the samples exceeds the MDA and detection limit. The tracer yield of sample 5642 RI Grizzly Filter and Beaker is below acceptance limits. The data is repOlted. Except as noted, the LCS, batch blank and sample results are within acceptance limits. Uranium-234, 235, 238 The FWHM of sample 5677, 5678 RI NYC Filters and Beaker exceeds acceptance criteria due to the high level ofanalyte in the sample. Broadening of the peaks is expected due to the low specific activity of the Uranium. The spectrum was resolvable. The achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to historical process knowledge. The sample activity exceeds the MDA and detection limit for three of the four samples. Data is accepted. Except as noted, the LCS, batch blank, sample and sample duplicate results are within acceptance limits. Gamma Spectroscopy Pb-21O The achieved MDA of the samples exceeds the detection limit due insufficient sample volume. Data is accepted. Except as noted, the LCS, batch blank, sample and sample duplicate results are within acceptance limits. Alpha Scintillation Radium-226 The achieved MDA exceeds the detection limit due to sample volume available for analysis. Sample activity exceeds MDNDL in two of the three samples. The tracer yield of samples 5677, 5678 RI NYC Filters and Beaker, 5679 R2 NYC Filters and Beaker were below acceptance limits. There is no more sample volume available for re-analysis. The batch QC is within acceptance limits and indicates the method is in control. Data is reported. Except as noted, the LCS, batch blank and sample results are within acceptance limits. TestAmerica Laboratories, Inc. 3 Denison Mines (USA) Corp February 4, 2011 [ certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically and for completeness, for other than the conditions detailed above. The Laboratory Manager or a designee, as verified by the following signature has authorized release of the data contained in this hard copy data package. Reviewed and approved: Erika Jordan Customer Service Manager TestAmerica Laboratories, Inc. 4 Drinking Water Method Cross References I r DRINKING WATER ASTM METHOD CROSS REFERENCES I I Referenced Method lsotope(s) TestAmerica Richland's SOP N EPA 901.1 Cs-134,1-131 RL-GAM-001 EPA 900.0 Alpha & Beta RL-GPC-001 EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002 EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002 EPA 903.1 Ra-226 RL-RA-001 EPA 904.0 Ra-228 RL-RA-001 EPA 905.0 Sr-89/90 RL-GPC-003 ASTM 05174 Uranium RL-KPA-003 EPA 906.0 Tritium RL-LSC-005 Results in this report relate only to the sample(s) analyzed, Uncertainty Estimation TestAmerica Richland has adopted the internationally accepted approach to estimating uncertainties described in "NIST Technical Note 1297, 1994 Edition". The approach, "Law of Propagation of Errorsll• involves the identification of all variables in an analytical method which are used to derive a result. These variables are related to the analytical result (R) by some functional relationship, R = constants * f(x ,y.z .... ). The components (x,y,z) are evaluated to determine their contribution to the overall method uncertainty. The individual component uncertainties (ua are then combined using a statistical model that provides the most probable overall uncertainty value. All component uncertainties are categorized as type A, evaluated by statistical methods, or type B. evaluated by other means. Uncertainties not included in the components, such as sample homogeneity, are combined with the component uncertainty as the square root of the sum~of~the-squares of the individual uncertainties. The uncertainty associated with the derived result is the combined uncertainty (u,) multiplied by the coverage factor (1,2, or 3). When three or more sampl e replicates are used to derive the analytical result, the type A uncertainty is the standard deviation of the mean value (Sl?n). where S is the standard deviation of the derived results. The type B uncertainties are all other rand om or non-random components that are not included in the standard deviation. The derivation of the general "Law of Propagation of Errors" equations and specific example are available on request. TestAmerica rp(Gcncralinfo v3.72 TcstAmeri ca Laboratories, Inc. 5 o. Action Lev Batch Bias COCNo Count Error (#s) Total Vncert (#s) "e_Combilled Ullcerfttillly. (#s), Coverage Factor CROL (RL) Lc Lot-Sample No MOqMOA Primary Detector Ratio U-234/U-238 Rs t/MOC RstfTotUccrt Report DB No RER SOG Sum Rpt Alpha Spec Rst(s) Work Order Yield TestAmerlca Report Definitions An agreed upon activity level used 10 trigger some action when the final result is greater than or equal to the Action Level. Often the Action Level is related to the Decision Limit. The QC preparation batch number that relates laboratory sa mples to QC samples that were prepared and analyzed together. Defined by the equation (ResultlExpccled)-1 as defined by ANS I N 13.30. Chain ofCuslody Number assigned by the Client or TestAmenca. Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same units as the result. For Liquid Sci ntillation Count ing (LSC) the batch blank count is the background. All known uncertainties associated with the preparation and analysis of the sample are propagated to give a measure of the uncertainty associated with the result, lie the combilled III/certainty. The uncertainty is absolute and in the same units as the result. The coverage factor defi nes the width of the confidence interval, 1,2 or 3 standard deviations. Contractual Required Detection Limit as defined in the Client 's Statement Of Work or TestAmerica ·'defau lt·, nominal detection limit. Often referred to the reporting level (RL) Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Vo lume associated with the sample. The Type I error probability is approximately 5%. Lc=( 1.645 * Sqrt(2*(BkgmdCnt/BkgmdCnt Min)/SCntMin)) * (ConvFctl(Eff*Yld*Abn*Vol) * IngrFct). For LSC methods the batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count is zero. The number assigned by the L1MS software to track samples received on the same day for a given client. The sample number is a sequential number assigned to each sample in the Lot. Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Vo lume with a Type I and II error probability ofapproximatcly 5%. MDC = (4.65· Sqrt«BkgmdCntlBkgmdCn,Min)/SCntMin) + 2.711SCn'Min) * (ConvFctl(Eff* Yld * Abn * Vol) *lngrFc'). For LSC methods the batch blank is used as a measure of the background variability. The instrument identifier associated with the anal ysis of the sample aliquot. The U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural uranium in NIST SRM 4321 C is 1.038. Ratio of the Result to the MDe. A value greater than I Illay indicate activity above background at a high level of co nfidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of2 a value greater than I may indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence interval. Caution should be used when applying this factor and it should be used in concert with the qualifi ers associated with the result. Sample Identifier used by the report system. The number is based upon the fi rst five digits of the Work Order Nu mber. The eq uation Replicate Error Ratio = (S-D)/[sqrt(TPUs2 + TPUd2)J as defined by ICPT BOA where S is the original sample result , D is the result of the duplicate, TPU s is the tota l uncertainty of the original sample and TPUd is the total uncertainty of the duplicate sample. Sample Delivery Group Number assigned by the Client or assigned by TestAmeri ca upon sample receipt. The sum of the reported alpha spec results for tests derived from the same sample excluding duplicate result where the results are in the same units. The L1MS software assign test specific identifier. The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method. rptCcncrallnfo v3.72 TestAmerica Laboratories, Inc. 6 Sample Results Summary Date: 04-Feb-11 TestAmerica Ordered by Method, Batch No., Client Sample 10. Report No. : 45715 SDG No: 42540 Client Id Tracer MOe or Batch Work Order Parameter Result +. Uncertainty ( 2s) Qual Units Yield MDA CRDL RER2 0355384 RICHRC5011 5642 R1 GRIZZLY FILTER & BEAKE MCFPL1AA TH-228 2.43E-08 +-B.OE-08 U UCI/SA 17% 1.13E-07 TH-230 B.Ol E-07 +-2.1E-07 UCI/SA 17% 8.19E-08 3.00E-15 TH-232 O.OOE+OO +-3.1 E-08 U UCI/SA 17% 8.19E-08 5676 BAG HOUSE FILTER & BEAKER MCFRJ1AA TH-228 2.93E-08 +-3.3E-08 U UCI/SA 34% 5.40E-08 TH-230 8.89E-OB +-1.7E-OB UCI/SA 34% 5.19E-08 3.00E-15 TH-232 1.13E-OB +-2.8E-07 UCI/SA 34% 5.19E-08 5677,5678 R1 NYC FILTERS & BEA MCFP51AA TH-228 1.09E-07 +-7.5E-08 UCI/SA 26% 7.28E-08 TH-230 1.30E-04 +-2.BE-05 UCI/SA 26% 1.02E-07 3.00E-15 TH-232 9.85E-OB +-2.1E-OB UCI/SA 26% B.99E-08 5679 R2 NYC FILTERS & BEAKERS MCFQ71AA TH-228 2.73E-08 +-2.0E-08 UCIISA 88% 2.23E-08 TH-230 5.38E-05 +-9.0E-OB UCIISA 88% 2.14E-08 3.00E-15 TH-232 7.34E-07 +-1.5E-07 UCI/SA 88% 2.14E-08 0355385 FFSR 5642 R1 GRIZZLY FILTER & BEAKE MCFPL1 AC U-234 1.01 E-05 +-1.8E-OS U UCI/SA 92% 3.57E-05 9.00E-15 U-23S 5.05E-OB +-1.3E-05 U UCI/SA 92% 3.03E-05 9.00E-15 U-238 4.42E-05 +-3.7E-05 U UCI/SA 92% 4.BSE-05 9.00E-15 5676 BAG HOUSE FILTER & BEAKER MCFRJ1AE U-234 1.01 E-03 +-2.2E-04 UCI/SA 84% 3.09E-05 9.00E-15 U-235 3.Bl E-05 +-3.1 E-05 UCI/SA 84% 2.83E-05 9.00E-15 U-238 8.77E-04 +-2.0E-04 UCI/SA 84% 3.09E-OS 9.00E-1S 5677,5678 R1 NYC FILTERS & BEA MCFP51AE U-234 4.5BE-02 +-1.3E-02 UCI/SA 92% 3.72E-OS 9.00E-15 U-235 2.80E-03 +-8.BE-04 UCI/SA 92% 2.82E-OS 9.00E-1S U-238 4.74E-02 +-1.4E-02 UCI/SA 92% 3.72E-05 9.00E-15 5679 R2 NYC FILTERS & BEAKERS MCFQ71AE U-234 4.18E-02 +-B.BE-03 UCI/SA 95% 4.B2E-05 9.00E-15 U-235 1.39E-03 +-3.0E-04 UCI/SA 95% 3.51 E-05 9.00E-15 U-238 4.2BE-02 +-B.7E-03 UCI/SA 95% B.55E-05 9.00E-15 0355382 RICHRC5011 TestAmerica REIU -Replicate Error Ratio "" (S-D)/lsqrt(sq(TPUs)+sq(TI'Ud»l as defined by IClyr BOA. rptSTlRchSaSum U Qual - Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda, Total Um:crl,CllDL, or not mary2 VS.2.10 identified by gamma scan software. A2002 TestAmerica Laboratories, Inc. 7 Sample Results Summary Date: 04-Feb-11 TestAmerica Ordered by Method, Batch No., Client Sample ID. Report No. : 45715 SDG No: 42540 Client Id Tracer MOe or Batch Work Order Parameter Result +-Uncertainty ( 25) Qual Units Yield MDA CRDL 0355382 RICHRC5011 5676 BAG HOUSE FILTER & BEAKER MCFRJ1 AD Pb-210 5.25E-07 +-2.5E-07 UCI/SA 97% 3.92E-07 6.00E-14 5677,5678 R1 NYC FILTERS & BEA MCFP51AD Pb-210 2.21 E-05 +-3.9E-06 UCI/SA 52% B.37E-07 6.00E-14 5679 R2 NYC FILTERS & BEAKERS MCFQ71AD Pb-210 1.B7E-05 +-3.2E-06 UCI/SA 86% 4.70E-07 6.00E-14 0355383 RL-RA-001 5676 BAG HOUSE FILTER & BEAKER MCFRJ1AC RA-226 7.72E-OB +-1.0E-07 U 100% 1.9SE-07 9.00E-14 5677,5678 R1 NYC FILTERS & BEA MCFPS1AC RA-226 S.92E-07 +-S.3E-07 U 17% 9.21 E-07 9.00E-14 5679 R2 NYC FILTERS & BEAKERS MCFQ71AC RA-226 1.49E-06 +-6.6E-07 14% 7.10E-07 9.00E-1 4 No. of Results: 30 TestAmerica U.EH2 -Hcplicatc Error Halio = (S-D)/lsqrt(sq(TPUs)+sq(TPUdHl as defined by le lYJ' UOA. rptSTLRchSaSum mary2 V5.2.10 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less th an the Mdc/Mda, Total Unccrt,CnOL, or not identified by gamma scan software. TcstA mcrica Laboratories, Inc. 8 RER2 QC Results Summary Date: 04-Feb-11 TestAmerica Ordered by Method, Batch No, QC T ype,. Report No. : 45715 SDG No.: 42540 Batch Tracer LCS Work Order Parameter Result +-Uncertainty ( 25) Qual Units Yield Recovery Bias MDClMDA RICHRC5011 0355384 BLANK QC, MCM5K1AA TH-22S -6.25E-09 +-1.SE-08 U UCI/SA 34% 4.60E-OS TH-230 4.00E-08 +-4.5E-08 U UCI/SA 34% 6.86E-OS TH-232 1.14E-OS +-2.3E-OS U UCI/SA 34% 4.20E-OS 0355384 LCS, MCM5K1AC TH-230 2.43E-06 +-4.5E-07 J UCI/SA 52% 107% 0.1 2.45E-08 FFSR 0355385 BLANK QC, MCM5V1AA U-234 3.99E-OS +-9.6E-OS U UCI/SA 92% 2. 17E-07 U-235 -7.60E-09 +-9.6E-OS U UCI/SA 92% 2. 17E-07 U-23S -7.60E-09 +-9.6E-OS U UCI/SA 92% 2. 17E-07 0355385 LCS, MCM5V1AC U-234 5.56E-06 +-1.3E-06 UCI/SA 86% 103% 0.0 2.10E-07 U-235 2.53E-07 +-2.1E-07 UCI/SA 86% 102% 0.0 1.70E-07 U-238 6.15E-06 +-1.4E-06 UCI/SA 86% 108% 0.1 2.10E-07 RICHRC5011 0355382 BLANK QC, MCM451AA Pb-210 3.99E-07 +-3.5E-07 U UCI/SA 72% 5.96E-07 0355382 LCS, MCM451AC Pb-210 1.11 E-05 +-1.9E-06 UCI/SA 79% 123% 0.2 5.04E-07 RL-RA-001 0355383 BLANK QC, MCM491AA RA-226 6.06E-OS +-S.4E-OS U 99% 1.56E-07 0355383 LCS , MCM491AC RA-226 S.23E-06 +-1. 7E-06 J 100% 82% -0.2 9.90E-OS No. of Results: 14 TestAmerica Hias -(Result/Expected)-l as defined by ANSI NI3.30. rptSTLRchQcSum maryV5.2.10 A2002 J Qual-No UI< qualifier has been assigned and the result is below the Reporting Limit, RL (ClWL) or Report Value is Estimated. U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda, Total Unccrt,CRDL, or not identified by gamma scan software. TcstAmerica Laboratories, Inc. 9 FORM I Date: 04-Feb-11 SAMPLE RESULTS Lab Name: T estAmerica SDG: 42540 Collection Date: 10/19/2010 9:30:00 AM Lot-Sample No.: JOL160499-1 Report No. : 45715 Received Date: 1211 5/2010 11:00:00 AM Client Sample ID: 5642 R1 GRIZZLY FILTER & BEAKE COC No.: Matrix: FILTER Denison Mine 2010 4th Quarter Ordered b~ Client Samele ID, Batch No. Result Count Total MDClMDA, Rpt Unit, Yield RstfMDC, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 sl Uncert( 2 sl Action Lev Lc CRDL(RL) RstiTotUcert Prep Date Size Size Detector Batch: 0355384 RICHRC5011 Work Order: MCFPL 1AA Report DB 10: 9MCFPL10 TH-228 2.43E-08 U 6.0E-08 6.0E-08 1.13E·07 Uel/SA 17% 0.22 1/17/11 03:58 p 1.0 0.9B775 ALP171 4.00E-OB 0.81 Sample Sample TH-230 6.01E-07 1.7E-07 2.1 E-07 8.19E·OB Uel/SA 17% (7.3) 1/17/11 03:58 p 1.0 0.9B775 ALP171 2.59E-08 3.00E-15 (5.8) Sample Sample TH-232 O.OOE+OO U O.OE+OO 3.1 E-OB 8.19E-OB Uel/SA 17% O. 1/17/11 03:58 p 1.0 0.9B775 ALP171 2.59E-08 O. Sample Sample Batch: 0355385 FFSR Work Order: MCFPL 1AC Report DB 10: 9MCFPL 10 U·234 1.01 E-05 U 1.8E-05 I .BE-05 3.57E-05 UCI/SA 92% 0.28 1/21 /1103:21 p 1.0 0.00096 ALP5 9.30E-06 9.00E-15 (1.1) Sample Sample U-235 5.05E-06 U 1.3E-05 1.3E-05 3.03E-05 Ue l/SA 92% 0.17 1/21/11 03:21 p 1.0 0.00096 ALP5 6.58E·06 9.00E-15 0.78 Sample Sample U·238 4.42E-05 U 3.6E-05 3.7E-05 4.65E·05 UCI/SA 92% 0.95 1/21/11 03:21 p 1.0 0.00096 ALP5 1.47E·05 9.00E-15 (2.4) Sample Sample Ratio U-2341238 = 0.2 No. of Results: 6 Comments: TestAmerica MDCIMDA,Lc - Detection, Decision Level based on instrument background or blank. adjusted by the sample Efficiency, Yield, and Volume. rptSTlRchSample J Qual -No UI< qualifier has been assigned and the result is below the Reporting Limit, Rl (CROll or Report Value is Estimated. VS.2.10 A2002 U Qual -Analyzed for but not detected above limiting criteria. limit criteria is less than the MdcJMda, Total Uncert,CROl, or not identified by gamma scan software. TestAmerica Laboratories, Inc. 10 FORM I Date: 04-Feb-1 1 SAMPLE RESULTS Lab Name: TestAmerica SDG: 42540 Collection Date: 121BI2010 9 :30:00 AM Lot-Sample No.: JOL 160499-4 Report No.: 45715 Received Date: 12/1 5/201011 :00:00 AM Client Sample 10: 5676 BAGHOUSE FILTER & BEAKER COC No.: Matrix: FILTER Denison Mine 2010 4th Quarter Ordered b~ Client Sam~le 10, Batch No. Result Count Total MOCIMOA, Rpt Unit, Yield RstlMDC, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 25) Uncert( 2 5) Action Lev Lc CROLIRL) RsVTotUcert Prep Date Size Size Detector Batch: 0355382 RICHRC5011 Work Order: MCFRJ1AD Report DB 10: 9MCFRJ10 Pb-210 5.25E-07 2AE-07 2.5E-07 3.92E-07 UCI/SA 97% (1.3) 1/27/11 OB:51 a 1.0 0.98845 GPC31D 1.91 E-07 6.00E-14 (4.1) Sample Sample Batch: 0355383 RL-RA-001 Work Order: MCFRJ1AC Report DB 10: 9MCFRJ10 RA-226 7.72E-OB U 1.0E-07 1.0E-07 1.95E-07 100% 0.4 1/25/11 03:00 p 1.0 0.9884 ASC4HB B.96E-OB 9.00E-14 (1.5) Sample Sample Batch: 0355384 RICHRC5011 Work Order: MCFRJ1AA Report DB 10: 9MCFRJ10 TH-228 2.93E-OB U 3.3E-OB 3.3E-OB 5AOE-OB UCI/SA 34% 0.54 1/17/11 03:5B p 1.0 0.9884 ALP175 1.71 E-OB (1.8) Sample Sample TH-230 B.B9E-06 5.0E-07 1.7 E-06 5.19E-OB UCIISA 34% (171.5) 1117/11 03:5B p 1.0 0.9884 ALP175 1.64E-OB 3.00E-15 (10.3) Sample Sample TH-232 1.13E-06 1.BE-07 2.BE-07 S.19E-OB UCIISA 34% (21.7) 1/17111 03:5B p 1.0 0.9884 ALP175 1.64E-OB (82) Sample Sample Batch: 0355365 FFSR Work Order: MCFRJ1AE Report DB 10: 9MCFRJ10 U-234 1.01 E-03 1.6E-04 2.2E-04 3.09E-05 UCI/SA 84% (32.6) 1/21 /1103:21 p 1.0 0.00112 ALP211 7.0SE-06 9.00E-15 (9.) Sample Sample U-235 3.61 E-05 3.0E-05 3.1 E-05 2.B3E-05 UCI/SA 84% (1.3) 1/21 /11 03:21 p 1.0 0.00112 ALP211 S.76E-06 9.00E-15 (2.3) Sample Sample U-238 B.77E-04 1.5E-04 2.0E-04 3.09E-05 UCI/SA 84% (28.4) 1/21/11 03:21 p 1.0 0.00112 ALP211 7.05E-06 9.00E-15 (8.7) Sample Sample Ratio U-2341238 = 1.1 TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency. Yield, and Volume. rptSTLRchSample J Qual -No UI< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. VS.2.10 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda, Total Uncert,CRDL, or not identified by gamma scan software. TestAmerica Laboratories, Inc. II FORM I SAMPLE RESULTS Date: 04-Feb-11 Lab Name: TestAmerica Lot-Sample No.: J0L160499-4 SDG: 42540 Report No.: 45715 COC No.: Collection Date: 12/8/20109:30 :00 AM Received Date: 12/15/201011 :00 :00 AM Matrix: FILTER Client Sample 10: 5676 BAG HOUSE FILTER & BEAKER Denison Mine 2010 4th Quarter Ordered by Client Sample 10, Batch No. Result Count Parameter Qual Error ( 2 s) Total MDC1MDA, Rpt Unit, Uncert( 2 s) Action Lev Lc Yield RstfMDC, CRDL(Rl} RstfTotUcert Analysis, Prep Date No. of Results: 8 Comments: TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. J Qual -No UI< qualifier has been assigned and the result is below the Reporting Limit, RL (CROL) or Report Value is Estimated. Total Sa Size Aliquot Size rptSTLRchSample VS.2.10 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda, Total Uncert,CRDL, or not identified by gamma scan software. TestAmerica Laboratori es, Inc. 12 Primary Detector FORM I Date: 04-Feb-11 SAMPLE RESULTS Lab Name: TestAmerica SDG: 42540 Collection Date: 12/7/20108:00:00 AM Lot-Sample No.: JOL160499-2 Report No. : 45715 Received Date: 12/15/201011 :00:00 AM Client Sample 10: 5677,5678 R1 NYC FILTERS & BEA COC No.: Matrix: FILTER Denison Mine 2010 4th Quarter Ordered bl Client SamE Ie ID, Batch No. Parameter Batch: 0355382 Pb·210 Batch: 0355383 RA·226 Batch: 0355384 TH-228 TH-230 TH-232 Batch: 0355385 U-234 U-235 U-238 TestAmerica Result Count Total MDClMDA, Rpt Unit, Yield RstiMOC, Analysis, Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) RstITotUcert Prep Date RICHRC501 1 Work Order: MCFP51AD Report DB 10: 9MCFP510 2.21E-OS 9.9E-07 3.9E-06 B.37E-07 UCI/SA 52% (26.4) 1/27/11 OB:51 a 4.07E-07 6.00E-14 (11. 2) RL-RA-001 Work Order: MCFP51AC Report DB 10: 9MCFP510 5.92E-O? U S.2E-07 S.3E-07 9.21 E-07 17% 0.64 1/2S/11 03:14 p 4.13E-07 9.00E-14 (2.2) RICHRC5011 Work Order: MCFP51AA Report DB 10: 9MCFP51Q 1.09E-O? 7.1 E-08 7.SE-OB 7.2BE-OB UCI/SA 26% (1.5) 1/17/11 03:SB p 2.30E-OB (2.9) 1.30E-04 2.2E-06 2.6E-OS 1.02E-07 UCI/SA 26% (1267.5) 1/17/11 03:S8 p 3.83E-08 3.00E-1S (9.9) 9.BSE-06 6.1 E-07 2.1 E-06 6.99E-OB UCI/SA 26% (140.9) 1/17/11 03:SB p 2.21 E-OB (9.5) FFSR Work Order: MCFP51AE Report DB 10: 9MCFP510 4.S6E-02 1.0E-03 1.3E-02 3.72E-OS UCI/SA 92% (1 225.3) 1/21/1103:21 p 1.06E-OS 9.00E-1 S (6.8) 2.80E-03 2.6E-04 B.6E-04 2.B2E-OS UCI/SA 92% (99.3) 1/21/11 03:21 p 6.13E-06 9.00E-1S (6.5) 4.74E-02 1.1 E-03 1.4E-02 3.72E-OS UCI/SA 92% (1273.1) 1/21/11 03:21 p 1.06E-OS 9.00E-1S (6.8) Ratio U-2341238 -1.0 MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. J Qual-No UI< qualifier has been assigned and the resuH is below the Reporting Limit, RL (CROL) or Report Value is Estimated. Total Sa Aliquot Size Size 1.0 0.98877 Sample Sample 1.0 0.9888 Sample Sample 1.0 0.98877 Sample Sample 1.0 0.98877 Sample Sample 1.0 0.98877 Sample Sample 1.0 0.00107 Sample Sample 1.0 0.00107 Sample Sample 1.0 0.00107 Sample Sample rptSTLRchSample VS.2.10 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda, Total Uncert,CRDL, or not identified by gamma scan software. TestAmcrica Laboratories, Inc. 13 Primary Detector GPC31B ASC2HA ALP173 ALP173 ALP173 ALP6 ALP6 ALP6 FORM I SAMPLE RESULTS Date: 04-Feb-11 Lab Name: TestAmerica Lot-Sample No.: JOL 160499-2 SDG: 42540 Report No.: 45715 COC No.: Collection Date: 1217120108:00:00 AM Received Date: 12/15/201011 :00:00 AM Matrix: FILTER Client Sample 10: 5677,5678 R1 NYC FILTERS & BEA Denison Mine 2010 4th Quarter Ordered by Client Sample 10. Batch No. Result Count Parameter Qual Error ( 251 No. of Results: 8 Comments: Total MDCIMDA, Rpt Unit, Uncert( 2 5) Action Lev Lc Yield RstlMDC, CRDL(RLJ RstITotUcert Analysis, Prep Date TestAmerica MDCIMDA.Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. Total Sa Size Aliquot Size rptSTLRchSample J Qual -No UI< qualifier has been assigned and the result is below the Reporting limit, Rl (CROll or Report Value is Estimated. VS.2.10 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda, Total Uncert,CRDL, or not identified by gamma scan software. TestAmerica Laboratories, Inc. 14 Primary Detector FORM I Date: 04-Feb-11 SAMPLE RESULTS Lab Name: TestAmerica SDG: 42540 Collection Date: 1218/20108:00:00 AM Lot-Sample No.: JOL 160499-3 Report No. : 45715 Received Date: 12/15/201011:00:00 AM Client Sample 10: 5679 R2 NYC FILTERS & BEAKERS COC No.: Matrix: FILTER Denison Mine 2010 4th Quarter Ordered b~ Client Samele ID, Batch No. Result Count Total MOCIMOA, Rpt Unit, Yield RstJMDC, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2S) Uncert( 2 51 Action Lev Lc CRDL(RL) RstITotUcert Prep Date Size Size Detector Batch: 0355382 RICHRC5011 Work Order: MCFQ71AD Report DB 10: 9MCFQ710 Pb-21 0 1.87E-05 6.4E-07 3.2E-06 4.70E-07 UCI/SA 86% (39.8) 1/27/11 08:51 a 1.0 0.98899 GPC31C 2.29E-07 6.00E-14 (11.7) Sample Sample Batch: 0355383 RL·RA-001 Work Order: MCFQ71AC Report DB 10: 9MCFQ710 RA·226 1.49E-OS S.9E-07 S.6E-07 7.10E-07 14% (2.1) 1/2S/11 03:13 p 1.0 0.989 ASC3MA 2.97E-07 9.00E-14 (4.S) Sample Sample Batch: 0355384 RICHRC5011 Work Order: MCFQ71AA Report DB 10: 9MCFQ710 TH·228 2.73E-08 1.9E-08 2.0E-08 2.23E-08 UCI/SA 88% (1.2) 1/17/11 03:58 p 1.0 0.98899 ALP174 7.0SE-09 (2.8) Sample Sample TH·230 S.38E-OS 7.9E-07 9.0E-OS 2.14E-08 UCI/SA 88% (2S12.2) 1/17/11 03:S8 p 1.0 0.98899 ALP174 S.77E-09 3.00E-1S (12) Sample Sample TH-232 7.34E-07 9.3E-08 1.SE-07 2.14E-08 UCI/SA 88% (34.2) 1/17/11 03:S8 p 1.0 0.98899 ALP174 S.77E-09 (9.6) Sample Sample Batch: 0355385 FFSR Work Order: MCFQ71AE Report DB 10: 9MCFQ710 U-234 4.18E-02 1.1E-03 S.SE-03 4.S2E-OS UCI/SA 95% (903.7) 1/21/11 03:21 p 1.0 0.00089 ALP7 1.32E-OS 9.00E-1S (12.7) Sample Sample U·235 1.39E-03 2.0E-04 3.0E-04 3.S1E-OS UCI/SA 95% (39.7) 1/21/11 03:21 p 1.0 0.00089 ALP7 7.S2E-OS 9.00E-1S (9.4) Sample Sample U-238 4.2SE-02 1.1 E-03 S.7E-03 S.SSE-OS UCI/SA 95% (650.6) 1/21/11 03:21 p 1.0 0.00089 ALP7 2.29E-OS 9.00E-1S (12.7) Sample Sample Ratio U-2341238 -1.0 TestAmerica MDCIMDA.Lc -Detection, Decision level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual-No U!< qualifier has been assigned and the result is below the Reporting Limit. RL (CRDL) or Report Value is Estimated. V5.2.10 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda, Total Uncert,CRDL. or not identified by gamma scan software. TestAmerica Laboratories, Inc. 15 FORM I SAMPLE RESULTS Date: 04-Feb-11 Lab Name: TestAmerica Lot-Sample No.: JOL 160499-3 SDG: 42540 Report No.: 45715 cac No.: Coliection Date: 12/8/201 0 8:00:00 AM Received Date: 12/15/20101 1:00:00 AM Matrix: FILTER Client Sample 10: 5679 R2 NYC FILTERS & BEAKERS Denison Mine 2010 4th Quarter Ordered by Client Sample 10, Batch No. Result Count Parameter Qual Error ( 25) No. of Results: 8 Comments: Total MDClMDA, Rpt Unit, Uncert( 2 s) Action Lev Lc Yield RstlMDC, CRDL(RL) RstlTotUcert Analysis, Prep Date TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank. adjusted by the sample Efficiency, Yield, and Volume. Total Sa Size Aliquot Size rptSTLRchSam Ie J Qual -No UI< qualifier has been assigned and the result is below the Reporting Limit. RL (CROLl or Report Value is Estimated. VS.2.10 A2002 P U Qual-Analyzed for but not detected above limiting criteria. limit criteria is less than the Mdc/Mda, Total Uncert,CRDL, or not identified by gamma scan software. TestAmerica Laboratories, Inc. 16 Primary Detector FORM II Date: 04-Feb-11 BLANK RESULTS Lab Name: T estAmerica SDG: 42540 Matrix: FILTER Report No.: 45715 Count Total MDCJMDA. Rpt Unit, RstlMDC, Analysis, Total Sa Aliquot Primary Parameter Result Qual Error ( 25) Uncert( 2 s) Lc CRDL Yield RstiTotUcert Prep Date Size Size Detector Batch: 0355382 RICHRC5011 Work Order: MCM451AA Report DB 10: MCM451AB Pb-210 3.99E-07 U 3.5E-07 3.5E-07 5.96E-07 UCI/SA 72% 0.67 1/27111 08:51 a 156.38 156.38 GPC32A 2.90E-07 6.00E-14 (2.2) Sample Sample Batch: 0355383 RL-RA-001 Work Order: MCM491AA Report DB 10: MCM491AB RA-226 6.06E-08 U 8.3E-08 8.4E-08 1.56E-07 99% 0.39 1/25/11 03:12 p 156.38 156.38 ASC5HA 7.04E-08 9.00E-14 (1.4) Sample Sample Batch: 0355385 FFSR Work Order: MCM5V1AA Report DB 10: MCM5V1AB U-234 3.99E-08 U 9.6E-08 9.6E-08 2.17E-07 UCI/SA 92% 0.18 1/21/11 03:22 p 1.0 0.15 ALP212 4.42E-08 9.00E-15 0.83 Sample Sample U-235 -7.60E-09 U 9.6E-08 9.6E-08 2.17E-07 UCIISA 92% -0.04 1/21/1103:22 P 1.0 0.15 ALP212 4.42E-08 9.00E-15 -0.16 Sample Sample U-238 -7.60E-09 U 9.6E-08 9.6E-08 2.17E-07 UCI/SA 92% -0.04 1/21/11 03:22 p 1.0 0.15 ALP212 4.42E-08 9.00E-15 -0.16 Sample Sample Ratio U-2341238 = -5.2 Batch: 0355384 RICHRC5011 Work Order: MCM5K1AA Report DB 10: MCM5K1AB TH-228 -6.25E-09 U 1.8E-08 1.8E-08 4.60E-08 UCI/SA 34% -0.14 1/1711103:58 p 1.0 1.0 ALP176 1.45E-08 -0.71 Sample Sample TH-230 4.00E-08 U 4.4E-08 4.5E-08 6.86E-08 UCIISA 34% 0.58 1/17/11 03:58 p 1.0 1.0 ALP176 2.66E-08 3.00E-15 (1.8) Sample Sample TH-232 1.14E-08 U 2.3E-08 2.3E-08 4.20E-08 UCI/SA 34% 0.27 1/17/11 03:58 p 1.0 1.0 ALP176 1.33E-08 1. Sample Sample No. of Results: 8 Comments: M DClMDA.Lc ~ Detection, Decision level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. TestAmerica rptSTLRchBlank V5.2.10 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda, Total Uncert,CRDL, or not identified by gamma scan software. TestAmerica Laboratories, Inc. 17 FORM II LeS RESULTS Lab Name: TestAmerica Matrix: FILTER Count Total Report Expected Parameter Result Qual Error ( 2 s) Uncert( 2 s) MDCIMDA Unit Yield Expected Uncert Batch: 0355382 RICHRC5011 Work Order: MCM451AC Report DB 10: MCM451CS Pb·210 1.11E-05 5.5E-07 1.9E-06 5.04E-07 UCI/SA 79% 9.06E-06 4.56E-07 Rec Limits: 20 115 Batch: 0355383 RL-RA-001 Work Order: MCM491AC Report DB 10: MCM491CS RA-226 B.23E-06 4.3E-07 1.7E-06 9.90E-OB 100% 1.01 E-05 1.04E-07 Rec Limits: 70 130 Batch: 0355385 FFSR Work Order: MCM5V1AC Report DB 10: MCM5V1 CS U-234 5.56E-06 9.7E-07 1.3E-06 2.10E-07 UCIISA 86% 5.42E-06 1.6BE-07 Rec Limits: 70 130 U-235 2.53E-07 2.1 E-07 2.1E-07 1.70E-07 UCI/SA 86% 2.47E-07 7.67E-09 Rec Limits: 70 130 U-238 6.15E-06 1.0E-06 1.4E-06 2.10E-07 UCI/SA 86% 5.6BE-06 1.76E-07 Rec Limits: 70 130 Batch: 0355384 RICHRC5011 Work Order: MCM5K1AC Report DB 10: MCM5K1 CS TH-230 2.43E-06 1.BE-07 4.5E-07 2.45E-OB UCI/SA 52% 2.28E-06 4.63E-08 Rec Limits: 70 130 No. of Results: 6 Comments: TestAmerica Bias -(RcsultlExpected)-l as defined by ANSI NI3.30. rptSTLRchLcs V5.2.10 A2002 TestAmerica Laboratories, Inc. 18 Date: 04-Feb-11 SDG: 42540 Report No.: 45715 Recovery, Analysis, Aliquot Primary Bias Prep Date Size Detector 123% 1/27/11 OB:51 a 151.62 GPC328 0.2 Sample 82% 1/25/11 03:13 p 151.62 ASC6MA -0.2 Sample 103% 1/21111 03:22 p 0.18 ALP213 0.0 Sample 102% 1/21/11 03:22 p 0.18 ALP213 0.0 Sample 108% 1/21/11 03:22 p 0.18 ALP213 0.1 Sample 107% 1/1 7/1103:58 p 1.0 ALP177 0.1 Sample ;;' ~ ;;; 3 " ~ ~r i ~ ;;. "~ ;;- f' -a III 1IIIIIIitUIIIIIIIUli 11111 JOL160499 Chain of Custody Record TemperaW19 on Receipt __ _ Drinking Water? Yes 0 No 0 TestAmerica THE LEADER IN ENVIRONMENTAL TESTING ~ ~82397 CfDL 160 491 '. JT:j3-L-f2:SYO TAL ... 4.J24 (l0071 Cl'Bm ! Project It.ansaer Tetco • ! Dean Ki'tchen Date 11112/1012010 i"'-""'''''''NUmbei ' [yjfl~ /-I2-lt Address r:-:::-:---"I T616PMn& Number Wea codsin=iix Nurrifiiii L~~.~~a~t 620 South , ! 8Ql-492-910J; 1 I Page of WN-.,. City ! ~ I StaIB L ZO_Co.t1e sie Coot2ct I Lab CGntact Analysis (Attach list if I American Fork I LUL 1IJ~400J ScottOrint_II.R'pnP,*,", I ~orsspacelSneed9d) Prof," ~-,miLoes>on IS • ." """""Wa,,.,Y Noo_ II i! r ill I I Denoson Mine 2010 4th Quarter . " CCfIlmctlPlJrcIlage O/doItQuots No. [ , I ~I [ Sampfe 1.0. No. and D8SCIipr/on . I Date Time (ContaIne1S lor each ~~ m2y be combined on cne fne) I ;7( i AI.atriX o ~ N I .., i .... -a! ~ ":' .,: '" .. '1 0: -II ; 5642 R1 Gduiy filt~'-andbeak",' ,-:~,-JIIO/1S/1o.,lts'30 .l X ! 1 .xX:·· VI , (E '1"1'::: r- IWJ<R1 NYC filte,,;nd beaker -L.;\t,.·,~ U/7/10 ]~~ xl I ! )\~l K1IXJI r\( '::" f-'r::::: l~67SR2NYCfi~er~andbeak~: 1.E'\~) ',2/S/,0 li s,Oo i xl ! I ~!Xlli;( '11:t ,1 Special Instruc:tJonSl Conditions of Recmpt ; 56768aghouseF;ite;and beaker -L'2[S/!0 -lJl9:3Ol x1 I I ! JlI{i'<l~ i /LC .. .:E a.:.i I I 1IIIIIII i ll illl ll l l'lfTrri'J Possible HamId ld$ntitiCBfion o Non-liJZtJtr1 0 Flammable o Skin Irrftsnt TUm -ArotJr/d time R9tJpfieii T I I TTl I ! I I I I I I I I ! 1 ! i i , -.l -.l IStt!TlPIe Dis;xJMJ o Poison 9 . 0 UnktlOllm 0 Retum To Client fA {(fa may be ~ed if SOfr'I{ies llJe rett!ined o DisposaIB'/Lab 0 Archive For ___ Months IongQltMn 1 mt:JI)fb) • QC P.oquitOfTl61l7ts (Specify) o 24 ~ 0 48 Houts 0" £lays 014 Days o 21 Days 0 Ot:her as Der.methoU I . ,.,...-, {M-"?'~-7 L.£. -1 /' 7> i 2. Re/inquisll4d8f~ -!-T!-~'~ . In Tan. II. 13 liD i ~ r>-y,-. ?J/b't ~fIf' . -z-ld.2T.67/ 1""'" ·1_ r R..,,_ By u u ~ I ""e I Tfme 'a'R~d~"~"~"'~d~By~---------------------------------JI'Da~"~------I~"r-~~-----4t'·a'R"~~"'~oByC--------1~8 ITnn8 Comments When Complete Email to:DeanorPaultetco@tetco-ut.com DISTRIBUTION: WHITe· RewmBd to cr.enl r.i/h Report-CANARY-Says with ~ 5amprv. FINK -FIe/a Copy TestAmerica rro.Mlj'!I'D'I@G!jiiiQ~e·!ffigil"t"'E'i-ViP ... ~ Sample Check-in List Date.Ti:oe Roo,;."",: 12/5 -I 0 ~ IIftlrJ GM Screen Result (om) I [3 (On), S' b.il~ ciiec~ , SDG #: L/2 s<I 0 ~f-l) SA; ~:-----,.r6~ Work Oder "iumber;;;;o! J..8O. ~ Chain of C"stocy # ______________ _ S':li?:o:.:og Co~<Zir.er ill: ~ j Air Bill # _________________ -~ 1. Kc C::st0dy Seal [ 1. Custod.y Seals d.z.ted and sig:1ed? 'So ClS~ody Sec.l [ Chain of Cus\.Ociy :e::.ord p~ese;}t? Cooler lemperature: ___ N.~ 5.Venniculite/packing materials is NA [ ) \Vet [ Ii.e::::::5 ~brough 10 for saL"'1ples. Initial appropriate response. 6 . Number of samples in shipping cOD.t2.iner (Each sample mey contain multiple botdeS): __ ~-I---"'-_____ _ 7. Sample holding limes exceeded? NA [ ) Yes [ ) N<lJ{)l ~~:p~ve: ;f.:-hazard labels III 11111\\ 111\111111 11\111 II III __ custody seals i) --e--appropriate sample labels )0[160499 3Z)1::~ in good conditio 4J;/eJ;y I __ are leaking __ are broken ~ __ have air bubbles (Only for samples requiring no head spac! 8. 9. 10. Sample pH appropriate for analysis requested Yes [ ) No [ ) N/~!Note discrepancies in #13) (If acidification necessary, then document sample ID, initial pH: ;;;"\ln~f~fHN03 added and pH after addition) 11. RPLID # of preservative used : ________________ .--, ___________ _ :Rs6 No [ Sample Location, Sample Collector Listed? + *For docwnentation only. No corrective aC1ion needed. 12. Were any anomalies identified in sample receipt? 13. Description of anomalies (include sample numbers): NA [ ) Se er side for additional comments Ilmr\.., , Sample Custodian: -'-'=='--?;;<......""-'--I-'-'n"""'(,"'Ct::::/o_~-='--____ .Date: /'2' IJ.I0PfL-£.Q Client Informed on ________ by __________ Person contacted _________ _ 9(f No action necessary; pr~cess as is PTOjec(Manager £~Q, C#1~='-=12q.(i.<-2A~0i4-(6-u----- LS-023, Rev. 12, 1011 0 TcstAmerica Laboratories, Inc. 20 APPENDIXD North Yellow Cake Scrubber Figure 1. Facility Schematic Representation Yellow Cake Dryer Baghouse Figure 2. Facility Schematic Representation Grizzly Baghouse Figure 3. Facility Schematic Representation Production Data (Retained by Denison Mines) D Facility: Denison Mines t (J. ~ y Stack Identification North Yellow Cake Scrubber 1~0-+1 , , p a: Distance upstream from next disturbance, feet --- p: Distance downstream from last disturbance, feet y: Distance of Sample Level to Ground, feet ____ ::: 0: Stack Inside Diameter, inches ____ '- Estimated Moisture, percent Estimated Temperature, of ___ .:...:..::.... Estimated Velocity, fpm ....:..". •• :..::.;'-__ _ Control Unit Type: Scrubber Number of Ports Figure I. Facility Schematic Representation Process Type: Yellow Cake Processing Facility: Denison Mines t CJ. ~ y Stack Identification: Baghouse 1+--0~1 [ a: Distance upstream from next disturbance, inches 57" istance downstream from laS1 disturbance, inches 4 54" y: Distance of Sample Level to Ground, feet 6 5' 0 : Stack Inside Diameter, inches 16" Estimated Moisture, percent 0-2% Estimated Temperature, of 125 p Estimated Velocity, fpm 1,400 Number efPorts 2 ---:::---=::: Control Unit Type: ~ Baghouse Figure 2. Facility Schematic Representation Process Type: Yellow Cake Processing Facility Denison Mines t a ~ y Stack Identification Grizzly Baghouse 1+-0 ~1 [ - p --- a: Distance upstream from next disturbance, inches 24.5" istance downstream from last disturbance, inches 48" y: Distance of Sample Level to Ground, feet 28' 0: Stack Inside Diameter, inches 18.75" Estimated Moisture, percent 1% Estimated Temperature, of Ambient Estimated Velocity, fpm 775 Number of Ports 2 Process Type: :::---=::: Control Unit Type: r--..L..------~I Ore Unloading and Conveyin ~ Baghouse Figure 3. Facility Schematic Representation Denison Mines Process Data Source: Grizzly 8aghouse Date: tD/;, /,;~) Time Tovl .s 7 rO 1-/ r: f "'" ";: ... tJ 1-4l? 00 gO /I O·Z. to: c.1o ::}-q $" rU 4:D I( o· z::.-. I a : 3<> 1-"i 40, D C,O 11 0. () I /)~ 00 1-c-,4 (S-TU l(().( 1·/ : 1> I.l 1-"1'1«6 I s~·& (D'1' ~ 1 Z.~<ro ·t'1~c.> Z--<{C;-((0 '0 Iz..' 3() t"1"l&->' &0 {1O .1:...8 '3 00 2[D4 10 y;-;r tI 0 . -z:. ('!>: ~ D jiQ;;>30 (Db (t 0·0 I V(:OO 't> O-u '-f V I -z. u l(lJ .l) 1'-f :3U i'0V(,,(j 1'( 0 (( () .c. {.,t;'. () () '6' ()C>l~ -ZoO I (d I IS.' 3 <) \3' DO c,,-t;-c:; /I 0, \ G ' «(J I • ~D \I <) o 5~ l[<l,-C, 16: 30 15()\)7~ 2-'$ J-110'~ /7: V(J '(0 1 50 !-ZO /1 () ,z. {t-~'5 D «DI?5 I L{ 0 ~ / u ,-r ~":OC1 \ 10 ' I Denison Mines Process Data Source: North Yellow Cake Date: /7-~ 7-I c/ Scrubber Flow GPM Time #1 #2 LIP 7:t.{~ "3~. « 't~S :, ... ·0 <;r:{)O (.~ l1· t ).0 <0: ~ 0 c,;.1-,-1. L( ~,0 -, ",:00 '6,-z...., 11· (" '" . 0 "1:30 'P. ?--11-' .... f )·0 I iJ: \\ () y ''S l;}' Cj 1'0 IO ;3() ~,) 11" .(; .;.0 W, D() Co'L-( 1-' '-f 5· !/ /1 :-;0 , ,Z:lJ'-> ('Z:,() J ~ ~/ I~~ ()O t6 . v( ( 1·'1 s·' '1 \ ~ : 30 'i' . '1..-\1·1 ; . ( l{' ()O I . cr,t. ( 1-. ti ,>.l,) I,-{:]O ). \ \ 1·) ,·0 (7: ()D V'.t q .. ~" 1·() \<;: ,0 eV\ It· (,p 7' !.) \(9:(/0 Ii 'S -\'l;'.( )·0 1(, ·)0 15·\0 ly.·1... 7' b If :'@o .\~~.(P \Y'7 )' i) l~: ~C> ~·G \~,'l. ? \:) I iI .~ .V Denison Mines Process Data Source: North Yellow Cake Date: Iz/y 00 Scrubber Fl ow GPM Time #1 #2 i1P '(j:50 «.(P I Y'~ ';·6 S-:--u u ~.lo vY,1 "1.0 $1-: :> 0 Sf' V lY'~ ~.() "1 : au y·ll (t,'"3 ~. { c'·30 «.(;, I <;.. "L "3 . c.,. tt):()O y' C ( y ' ~ -{ . ( lOt 3 v ((; (; 1'<' & , '3.0 I I: 0 /;) y·u Iy' \ ~~ .1 II : ,V ~'V 1 y'u 7'() ~: uO )-, ) 11-11 ).D I t.: ') \) £1>':' l 1,Ct> '3,0 1-; : ()O ~-..{ 1'1 ,'b' ~.b I'> : > 0 y.S-I ~-"" ~ ,( ,,-{ : DU c.--,c, l ~, ~ ~, () I<{.·,o y-GJ L c;'4 '->.0 ! <; . 00 ~i/'6 .t:' I c;r, ~ 7,0 v 7' ('-) .' 3D 'if ,v ~' l V') "}, 'I I (" ~ () v 11·1· (~,'-l ) \) 1(. '. 3J APPENDIXE Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature sensors were carried out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 4 Schematic of Method 51114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-test Dry Gas Meter Calibration Data Forms Type S Pitot Tube Inspection Data Sample Box Temperature Sensor Calibration E Schematic of Method 5/114 Sampling Train Thermocuple Duct wall l:'>'l \ \ Support Track \ tli, '" -Sampling Probe Support Chain Thermometer (i) rJ EJ r Vacuum Guage Heated \~~=~.' ~'~~~~5'j\ ::r:r nni~ --r-- Heated Filter Box -----' Check Valve Vacuum Line Sealed Flange /' Manometer ~ "2 • I! ~ , Exit I I Main !, Valve Metering ~ By-pass I Console I ~ Valve F igure 4 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket lhe e)Q)eCIed operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Ca6bralion Report), for a period of time necessary to achieve a rriniroom lolal volume of 5 cubic feel. 4) Record data and information in the GREEN cells, YELLOW cens are calculated, METERSERlAl':~ CRITICAL ORIFICE SET SERlAL .:~ EQUIPMENT 10': o o o RUN. 2 2 ~ FACTOR (AVG) 0.8137 0.8137 0.8137 0.5317 0.5317 0.5317 0.3307 0.3307 0.3307 TESTED VACUUM (in Hg) 13 151.813 13 162.2:58 13 169.470 13 ,"-... 13 189.289 13 194.938 13 200.502 13 21)5.782 13 211.040 USING THECRmcAl ORIFICES AS CALIBRATlON STANDARDS: 15&.719 169.470 174.828 189.289 , ... '" 200.214 205.782 211.040 216.30 6.906 7.212 5.358 5.241 5.6049 5.276 S.2ao 5.'" 5.260 72 " n " 72 70 72 .. 72 80 72 81 71 .. 71 81 71 82 .. 79 " 79 75 " SO .. " " " " 81 82 82 82 " " 79 81 " 82 82 " 82 " 83 DOM AVG 12.75 74.2.5 n.75 110.50 81.2.5 8>00 81.25 81.25 82.00 82.50 82.00 82.50 Facility FINAL ·';~-l ELAPSED TIME (MtN) e § ... 6.75 5.00 AVGIP ... ) 25.45 §90 ,go ,go § ... §." 8.00 1.20 7.50 1.20 1>0. 1>00 1>00 § .... .... .... New Calibration 2010 !:!ill 61147 !ill! lli2! ~ ~ ~ •. 3632 ~ IF YVARIATlON EXCEEDS 2.00%, ORIFICE SHOULD BE RECAllBRA TEO !.!ill !.2!!1 ~ AVG= ~ !&!!! 4.4014 AVG= ~ 4.3&41 ~ AVGz ~ U!1 ~ 2.!!! 1.J!2Z. Y!! 1.:!m 1.:!m 2.!!!! 1.005 .!:..22! 1.:!m 1 :2,g .2:l! P.dl The i:IIIowing equaJ:l1IS are used kl c:aIcuIate the standard wkmes of iii' passed through the DGM, V til (std). and the crilX:al om, V,,(std), and the DGM calbratiJn facDr, Y. These equations are ~ caIcuIaEd in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y -I 1.000 I') (2) (3) Vm("ill:= K,• Vm. Ph,w+ (6H 1\3.6) Tm Vert•H) Pbar. e ==K'· ~ '" Net volume of gas sample passed through DGM. corrected to standard conditions K," 17.64 "Rlin. Hg (English). 0.3858 "Klmm Hg (Metric) T .. = Absolute DGM~. temperature ('R -English.oK-Metric) = Volume of gas sample passed through the critical orifice. corrected to standard conditions T_ .. Absolute ambient temperature ('R. English. oK · Metric) K' '" A-.erage K' lador 110m Critical Ori6ee calibration y = VCI(<hf) V"'t.,dJ '"' DGM calibration factor Pre Calibration 200S AVERAGEAHg'f -1.628 , AH. '" (0.759) AH (V",(std1\ Vc,(std) v. J Temperature Sensors (4·2S'{)8) Reference In Out OF OF "F 34 73 125 36 73 124 35 74 125 1.Z!l! !,ill .lli! ~ .!:ill 1.630 1S1 1.539 :!.m METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meier wtlich brackellhe expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run al tested vacuum (from Orifice Calibration Report), for a period of lime necessary to achieve a minimum lolal volume of 5 cubic feel. 4) Recortl data and information in the GREEN eels, YELLOW cells are calculated. METER SERIAL': ZllltiJ CRIT1CAL ORIFICE SET SERIAL ':L-'C:='---" EQUIPMENT 10 II: K' TESTED TEMPERATURES "F INITIAL FACTOR VACUUM I DGM READINGS (Fr) I AMBIENT I DGMINLET.I DGMOUTLE~I DGM I ORFICE. I RUN . (AVG) (InHg) I INITIAL I FINAL I NET IV"" I 1N1W. Atw.. INll1AI. Fltw.. AVG o G G , l , 3 0.8137 0.8137 0.8137 0.5317 0.5317 0.5317 0.3307 0.3307 0.3307 13 190.80500 13 197.727 13 204.126 13 217.407 13 222.998 13 228.235 13 236.5510 13 241.1144 13 247.253 USING THE CRITICAL ORIFICES AS CAUBRATION STANDARDS: 197.727 204.126 210.564 222.998 228.235 234.505 241.844 247.253 252.885 6.912 6.399 6.438 5.591 5.237 6.270 5.293 5.409 5.632 72 72 74 72 7' 76 72 76 76 72 76 76 72 76 76 72 76 76 7. 76 76 7. 76 T7 74 77 T7 " 78 " " 78 79 78 78 79 78 " 82 " 79 " 78 79 78 75.5 77.25 78.15 77.00 77.25 77.25 77.00 77.50 77.75 FINAL G.~ ELAPSED TIME (MIN) • 6.50 6.00 6.00 a·DO 7.SO 9.00 AVG(P .... ) 25.5 10G.o:11 (1), I (In HJO) V .. (sTtl) §'" ~'" ~" 1.12 1.12 1.12 0.42 0.42 0.42 5.&615 5 4009 5.41&7 4.7012 4 4015 5.2696 44416 45348 47195 2010 Pre-Calibration IF Y VARIATION EXCEEOS 2.00%, ORIFICE SHOULD BE RECALIBRATEO 1 (2) I (3) IVA~:N~)~ Va (sTO) y ~ 53992 5.3992 AVG= ~ w.q 5.2920 AVG: 44716 4.5629 47454 AVG: 2.!!! :!.QQ9. 0.996 2.!!! .1.J!2! !An 1.&2! 1J!2! !.2QZ MQi Ull 1M§. ~ 2.:21 ~ Lm :t.lli 1.m! .Lill 1.ill !.ill 1.!!! 1Mi l.lli The {olawing equations are used to calculate the standacdvolumes of air passed through the DGM, V ... (Sid), and the critical orifice, V", (std), and the DGM calibration factor, Y. These equations are automaticaly calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 1.002 (1) (2) (3) Jlm(,,~ :: Ke • JIm. Pha/' + (611 /13.6) Tm Pba/" -e Ver{ .... ) = K'· .JTamb '" Net vokJme of gas sample passed through DGM. corrected to standard conditions K,: 17.64 "Rlin. Hg (English). 0.3858 "Klmm Hg (Metric) T"," Absolute OGM avo. temperature r R. English. oK· Metric} '" Volume of gas sample passed through the critical orifice, correded to standard conditions T _ : Absolute ambient temperature ("R. English. oK · Metric) K''' Average K' factor from Critical Orifice Calibration y = Vcr("d) Vml.,dl '" DGM calibration factor AVERAGE.4Hg=! 1.514 .4He '" (0.758)' AH (V",(std)) Vc,.{std) V", Temperature Sensors Reference In Out DF DF DF 3. 73 116 34 71 116 34 73 117 PRE Console #4 Calibration 2010 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of lime necessary to achieve a minimum total wlume of 5 cubic feel. 4) Record data and information in the GREEN cells, YEllOW cells are calculated. DATE: P""'''''-l METER PART #: ""==..:: METERSERIAL#:~ CRITICAL ORIFICE SeT SERIAL #: ~ EQUIPMENT 10 #: K' TESTED TEMPERATURES ·F FINAL 25.70 ELAPSED AVGIPt>o<) 25.70 2010 Pre-Calibration IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED ! FACTOR VACUUM I DGM READINGS (FT') I AMBIENTI DGM INLET. 1 DGM OUTL~ 1 OGM TIME(MIN) 10GM'~11 (1) 1 (2) 1 (3) IVA~;ON~)~ I ORIFICE If' I RUN. (AVG) (in Hg) I INITIAL I FlNAL I NET (V..) I INITIAL FINAL I<IITIAL fWAL AVG 9 (In H~O) Vm (STO) Vco (STD) y o G G 2 3 2 3 2 0.8137 0.8137 0.8137 0.5317 0.5317 0.5317 0.3307 0.3307 0.3307 13 164. ... 13 169.nO 13 175.087 12 197.702 12 210.703 12 216.011 12 181.2t120 12 , ........ 12 191.722 USING THE CRITICAL ORIFICES AS CAliBRATION STANDARDS: 169.770 175.087 180.451 2O~'" 216.011 221.324 186.454 191.722 196.990 ,.,.. 5.317 '.364 5.293 5.308 5.313 5.252 5.268 5.268 7' 7. 7. 7. 7. 7. 7. 7. 7. 63 .. .. 75 75 79 81 82 82 82 82 82 oo 81 81 82 82 81 .. .. 90 100 100 103 92 " " 97 97 .. 92 " " 96 .. 92 76.75 ,U, 89.25 87.50 89.00 89.75 87.00 88.50 87.75 §.oo '.00 '.00 3.00 3.00 3.00 § ... §.20 7.50 1.20 7.50 1.20 §Ae OAe OAe ~ ~ ~ ~ 4.4007 43989 4.3603 !ill! Yill !:m! !.m1 !.m1 AVG- ~ U363 4.4363 AVO;; 4..4147 ~ W.4! AVO- 1.22! l.ill .Lill l.ill 1..Q2! 1 .... 1.22! 1..Q2! 1.012 !&ll l.ill 1.012 .Q.gl :Y2 0.15 The fotJoNing equatbns are used locak:ulate the stan:lard 'oOOmes of air passed through the DGM, V .. (Sid), en::! the critical orifce, V., (sid), and the DGM calibration factor, Y. These equations are automaOCaI)' cat:ueted in the spreCKlsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y -I 1.010 (1) (2) (3) Vm("J) = K, .Vm -Pbar + (MI 113.6) Tm Pbar • e Ver C'oIl = K'· ...rr;;;;;; = Net \/OIume of gas sample passed through DGM, corrected to standard conditions K,;; 17.64 -Rlin. Hg (English), 0.3858 '"KImm Hg (Metric) T", '" Absolute DGM avg. temperature ~R • English. '"K. Metric) = Volume of gas sample passed through the critical orifice. corrected to standard conditions T _ '" Absolute ambient temperature ~R • English, '"K -Mettie) K';; Average K' factor from Critical Orifice Calibration Ve,;.",) y = --= DGM calibration factor Vmf •• 11 AVERAGE AHa =1 1.571 , AHa = (0.759) AH /y"",(SUJ») Vc.r(std) \ V", Temperature Sensors Reference In Out 'F 33 67 121 'F 34 66 120 'F 34 66 120 PRE Console #6 Calibration 2010 l.:ll! !.ill !.ill 1.&!M 1.600 !ill ll!J! !.ill 1.lli METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to caJibfate the dry gas meter which bracl<.et the expected operating range. 2) Record barometric pressure before and after calibration procedure. " iWW!gI ... !Wmll1ij~ b 4 r 3) Run at tested vacuum (from OrifICe Calibration Report). IOf a period of time necessary to achieve a minimum total volume of 5 cubic feet. Facility denison grizzly 4) Record data and information in the GREEN cells, YELLOW cells are calculated. K' TESTED FACTOR VACUUM RUN' {AVGI (in Hg) 0.5317 " 0.5317 " 0.5317_ 13 METER SERIAL #;c=J CRITICAL ORIFICE SET SERIAL #;~ EQUIPMENT 10 /I.: 105..603 110.977 110.977 116.400 116.400 122..201 5.374 5.423 5.001 70 56 1. 58 ,. S. 58 " SO 58 62 ,. S6 " .71_ 06. AVG 60.75 65.5 67.75 [:J, D:~~ D:~~ : lTIIIJ:: :: I I I I I I:: USING THE CRITICAl ORIFICES AS CAUBRAnON STANDARDS: ~ AVG!? .... ) 25.41 ElAPSeD TIME (MIN) e §., .. .... . ... 25.41 1.15 1.15 1.15 §§ §§ .un ~ ~ IF 'f VARlA.TION EXCEEDS 2.00%, ORIACE SHOULD BE RECALIBRATEO !JQ! ~ M2i AVG'" AVG= AVG= 1.011 .1Jlli 1.009 1.010 1 .... The Iolbwingequatiolls are used to calcu!ate\he staod3fd volumes of air passed througl\!he DGM, V,. {sk:l), and 1M critical orifice, Va (sid), and the DGM calibtationfaclof, Y. These equ300nsare alf.omatica/!ycalculated in the spreadsh~latxlVe. AVERAGE DRY GAS METERCAUBRATION FACTOR, Y = [1.01 0 I (1) 12) (3) Vm,.«Ij': K! .Vm. Pbar+(MII13.6) Tm ['bar·0 Vcrt."j) = K'· JTamb lilt Net volume of gas sample passed through DGM, corrected to standard com!itions Kl :: 17.64 ~in. HOI: (En>li:sh). 0.3555 "KImm Hg (Metric) TO''' Absolute DGM avg. tilmperature ("R -English, oK -Metric) = Volume of gas sample passed through the critical Orifice, corrected t::I standard conditions T_ = Ab~oIlP.e ambient t~erature'(R -Engllsh, "K . Mctri:;) VOi .ti) y: -- K' = Average K' facto( from Crit~1 Orifice Calib!lltion :: DGM calibration factor Vmj.I/l AVERAGE 6Ha :1'1.606 1 , &HI! = (0.159) .H (V",(Stdl) Vutstd) v", l..&n 1.604 t.m: postcalibration 2010 #3 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter whicll bracket the e:o:pected operating range. 2) Record barometric pressure before and atler caHbration procedure. t5 ellllllll_St'n"<'_Jidlllb"lf)~ ~~~ ~~ ji~ 3) Run at tested vacuum (from Orifice Calibration Repol1). for a period of time necessary to achieve a minimum total volume of 5 cu~c feet. 4) Rerord data and information in the GREEN cells, YELLOW cells are calculated. METERSERlAL.:lI CRITICAL ORlFlCE SET SERIAL #:~ eQUIPMENT 10 #: K· TESTED TEMPERATURES OF INITlAL Facility Dennison Baghouse FINAL AVG(Pt>or) 25.4' 25.45 IF YVARlATION EXCEEOS 2.00%. ORIFICE SHOULO BE RECALIBRATED ElAPSED 1 FACTOR VACUUM I OGM READINGS (FT' I AMBIENT 1 CGM INLET. 1 DGM OUTLE~ 1 OGM TIMEIMIN) 1 OGM ·~I I III 1 121 1 PI IV~~ON~)~ 1 ORIFICE /I. I RUN #I (AVG) (in Hg) I INITIAL I FINAL 1 NET(V"J I IN!TIAL F!NAL IN!TIAl.. FtW<L AVG • (in HzO) V .. ISTO) V",{STO) Y 0: 0.6317 14 925.202 930.742 0.6317 14 930.742 9_l6~ 0.5317 14 936.274 i41.817 D:E D:E~ USING THE CRITICAl ORIFICES AS CAUBRAnON STANDARDS: 5.540 7. 7. 7. 5.532 78 7S 74 '.543 78 7S 77 82 79 79 76 76 77 78 76 76.25 : I--u-r J] ]1 :: : I I I I I I:: §.oo 8.00 8.00 1.12 1.12 1.12 1.12 1.12 1.12 §§ §§ ~ !&ll ~ ~ ~ ~ AVG:: AVGa AVG = 1.000 LJlJM 1.221 .LQ!M 0.00 1.550 !.,ill. .till The foNowing equations are used to caicolatethe stn:lard vokJmes of air passed Ihrough the DGM, v" (sid), and the critical ortnce, Va (sld),.nj the DGM calibration facror, Y. These equati:lns are automaticaily ca!culaled in the spreadsheet above. AVERAGE ORY GAS METER CAUBRATION FACTOR, Y -r1"Jj04 I III (21 III Vm(s<4) = K, ... Vm" Pbar +(1lH 113.6) Tm Pbar • e Vcrl.,/d) = K· ... ~ = Net volume of gas sample passed through DGM, corrected te standard conditions I{, " 17 64 °Rlin. Hg (English). 0.3856 "KImm Hg (Metric) T ... = ~solu!e oGM ~wi. tempera~e tR -English. cK -Me!ric) c Volume of gas sample passed through the critical ori1ice. corrected to standard conditions T ..... :: Absolute ambioot temperature ('R -En!:;lish, "K -Maific) K' = AV'8I'agG K' facWr from Critical Orifi::.a Calibration Vc'! .. J) y. --= DGM calibration factor Vm,.k/j AVERAG .. H. =@s31 , Mia = (0.75 e) .o.H 1Y...",($tdl) Ycr(std) \ v'" postcaliOration 2010 #4 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Recofd barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), tor a periOd of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN celis, YElLOW cells are calculated. METER SERIAL.:~ CRITICAL ORIFICE SET SERIAL.:~ EQUIPMENT to ti: K' TESTED FACTOR VACUUM I ORIFICE!J RUN . lAVG) (inHg) 0.5317 13 412.102 0.5317 13 417.328 0.5317 13 422.573 417.328 422.573 427.344 5.226 5.245 5.271 " 7. " TEMPERATURES ·F 71 73 50 73 " 84 " 77 87 .. 07' " G D:§~ .0 .0 .0 1 1 1 1 1 1 D:EEJ ~ USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: .0 .0 .0 11_1 1 1 U 1 OGM AVG 77 79.75 81.75 0.00 0.00 0.00 0.00 0.00 0.00 FINAL. 25.45 eLAPSED nME(MIN) B AVG{P~.I 25.45 §.50 §.20 7.50 1.20 7.50 1.20 §§ §§ (1) V,. (STO) urn 4.3802 4.)856 Denison NYC IF Y VARIATION EXCeeOS 2.00%, ORIFICE SHOULD BE RECAlIBRATED 1 (2) (3) Iv_~~)~ Vu(STD) y ~ 1.001 1.651 ~ 1.003 ~ Yill ~ 1.537 AVG; 1.002 0.00 AVG= AVG'"' The fdlov.ing eQuations cr-e used b CCJIcuIaIe the sla<lda-tl volumes 01 air passed Ihroogh the DGM, V,. (sid), ald!he critical orifice, Vu (sid), and the OGfA calibration factor, Y. These eq!lltioos are automatically caIcu!aIad in IIle spre<dsheet aOOve. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y '" I 1.002 (1) 12) 13) Ym(,14') = K( -Ym-Pbar+(M 113.6) Tm Pbar .8 Vcr( •• ) = K'· ../Tamb = Net volume of gas sample passed through DGM, corrected to standard conditions KI II: 17.84 "RIin. Hg (Engtish). O.3858"K1mm H~ (Metric) T,., :. Absolute OGM avg. temperatlR rR -English, "K -Metric) '" Volume of gas sample passed through the critical orifice, corrected 10 standard conditions T _ = Absolute ambienf temperature ("R -English. "K -Mattie) K':. Av~ K' factor from Critical OrifiCe Calibration Yc,o;"., y:--:: DGM calibration factor Vm("., AVERAGE ..... =[ 1:644 -J ..... = (0.75 a )' ... 1'!..IStd)) Va(std) \ v .. Temperature Senso,", Refert!nce In Out OF <'f ~ 33 67 121 34 65 120 34 65 120 Pest test Console #e • 8:: ~ z ! t :: ~"' ~ ""-l.... B2 ]- , , w Type S Pitot Tube Inspection Data PiIO! Tube Idcntiric(llion: _--").."--7=L-_-_1..>= ______ _ Tl!chnician·_..:M-".'-'-M ...... ~ ... ,"~Ul"'''':!.Q''"'(C'"':A''--_______ _ D," • z..{V ;" 1'" ." ·35\ in. I'll"" ·?"n ;" u) < JOO a.= \ u: < 100 a,' I p, "---.:2..=--_ Z SO I25in. W s O.Q3 12Sin. W= .O'L€> in. W > 3 inches W::. 5 • i 'l.. in . Z > 3/4 inch Z= in. -'J<_~ .. ..-=' Y?: 3 inches L-~~ .-'!------ The pilOllubc m;.'cts Ihe specifications for a calibration fllclor of 0 84? \{ t., S Temperature Sensor Calibr;lIion Reference' ~ Temperature Temperature Tempcnllurc Source Reference Sensor Dirr ... rcncc t (Medium) ('F) ('F) (°F) AIR 1 1 11 ,0- Probe Continuity Ch,e.(lL -Y 'Ie. S Heat Check 248 -"'7-\Ie.~ d, 5 '+ AIR I I 1\ Iff ICE WATER 3'<-:'3 \ Slack OQILWATER <'0 '1 103 t SILICONE OIL y j PA t P. ,-' Type S Pitot Tube Inspection Data /--18 Pitot Tube! Id~milication: __ -=l7 _________ _ Technician: ___ '_'1_,_, --,M __ !:._, -'-N="""-'---''''<O'''-CC>-'--_____ _ r' D~ ."S7) in. P" ;; . 4:f~ in. 's P A = PB ? _-I::t-L..:;=::,'-;;-__ _ Is 1.05 • D, ~ D, s 1.50' D, ? __ ... 'j,,€..=S"'-__ _ PH = ,L{:)'"l in. • ClJ < [00 a,' 0 Cl] < lOG a~=: I p, =---'---- Z S; 0.125 in ,()O'" Z = ___ ,-"V,--_in. -e¥;':'~t-W W s;O.031 25 in. W = ,00 5 in. r- ! -+l ~~:. 14 W > 3 inches W = (" '/"L-in. _>-.. :~' 7/8 I·. Z > 3/4 inch Z= in. ' ... ~.~I ... +~nll , ! , , -."~~.,, .. ..-=~:i----y ~ 3 inches y = --=-3--'Y<4~_in , The pitot tube meeL~ the spcciticlllions for a calibrillion factor of 0.841 TCll1pc:ralure Sensor Clilibration Refcrcncc' [: Temperature rein rature Temperature Source Reference Sensor Diffcrellc~ /" I ;.;0' (Medium) C"Fl ("Fl (oF) AIR ('\5 (pI.. L Probe COlltinu ity --,' -7 \{e.S I-Ie-at Check 248 ---> '!<-S l.5'i AIR (.€> (,,9-I ICE WATER 3 '{ ~t.j @' Stack BOIL WATER '2. 0 'I 2 0'-1.- SILICONE OIL Type S Pitol Tube Inspection Data Dtllc: Pilot Tube Identification. _~ __ ,<_. -=c,,=-______ _ • J PA tee Dtc= ~tS-in . 1'", '" ~I 15-in. Po '" , ~I I S-in a. < 100 °1= <- 02 < 100 (12 '" 1- ~,~----- ~, ~---'---- ZS O.[25in. Z~ .OIC, in. -:CEfi?~ ._u_.L_. W W s 003125in. W= ,'''Z5 in. W > 3 inches W-(" in. Z > 3/4 ineh Z= in. +i-----y 2! 3 inches in. '111t! pilottubc met ts the srccifications for a calibration [actor 01'0 84? Y " Temperature Tent mture Temperature Sour.;e Rererence Sensor Difference l ", (Medium) ("F) !"f) ('FI AIR (pc, (,,~ <.) Probe ConliflllilV -'(-C S Htat Check 248 " YLC. 2-0 () AIR I • .:: (p, 0 [CEWATER :\ "1 3s () Stack DOlL WATER 17-<7.C: "l c:> s:-O SILICONE OIL TETeo Sample Box Temperature Sensor Calibration Oat" 11131201 0 Calibrator: Mike McNamara Reference: Omega CL3512A Temperature .ro Temp. Diff. Unit ID Thermocouple Source S~?~~)or or Result Location ; .. , ('F) ('F), PIF Oven Water 33 32 I Water 203 204 I A Probe Out Water 33 32 I Water 203 203 - Impinger Out Water 33 32 1 Water 2:03 202 I Oven Water 33 32 I water 203 204 I B Probe Out water 33 32 I Water 203 203 - lmpinger Out water 33 34 I Water 203 202 1 Oven Water 33 33 , Water 203 203 , C Probe Out Water 33 31 , Water 203 202 I Impinger Out Water 33 34 I Waler 203 202 I Oven Water 33 32 1 Water 203 203 - D Probe Out Water 33 32 I Water 203 203 - Impinger Out Water 33 34 I Water 203 202 I Oven Water 33 33 - water 203 204 I E Probe Out Water 33 33 - water 203 203 - Impinger Out Water 33 34 I water 203 201 2 Oven water 33 3'3 , Water 203 204 I F Probe Out Water 33 32 1 Water 203 203 , Impinger Out Water 33 33 , :~ 203 ~ I Impinger Out G I I Water 01 2 I Impinger Out H Water I l4 I Water 202 1 I Impinger Out I Water 33 33 - Water 203 203 - I Impinger Out J I Water 33 33 , Water 203 202 I APPENDIXF The testing followed the same procedures as outlined in previous protocols and tests at this facility. ATTACHMENT H SURFACE WATER GRAPHS AND FIELD DATA SHEETS 1.00E-05 1.00E-06 1.00E-07 ., OJ alI .OOE-OB '" o ::!.. 1.00E-09 ... ~ ~. • • • --1.00E-10 1.00E-11 0;'0'), ~" ~ Cottonwood Creek Dissolved Radionuclide Concentrations (uCi/ml) • • ~ • ~ -. • • • • • • • • • • ~ • • t ... •• A_ A •• •• .___ ___ -.. -._.-11 ••••. -... ~ ~"OJ rit-1' 0;0;'), ~" ,,<v" fll'O ~"Oj rit-'O [+!J-Nat. nh-230 ... Ra-226 f:l"-' ~ ~ ,," f:l0; ~ <,}"OJ • .-== .. a - 1.00E-06 1.00E-07 1.00E-08 ., iV ~.OOE-09 Cl o =- 1.00E-10 1.00E-11 1.00E-12 [b<O \,,0) ,,\" •• • •• • fIi. ~"O) ~1' Cottonwood Creek Suspended Radionuclide Concentrations (uCi/ml) • • • .. 2)1::> ~"q, rd-1' .. .. .. • 2)~ ~"q, ny'),<::! .. • • • • . .. • • 2)<0 ~"q, ~,,':l ,,'V • • • • • 2)'0 ~"q, ~,,<::! • • •• r:," ~ rd-'O • U-Na!. _ Th-230 .. Ra-226 • • .. . ... __ ..... -....-. I::>~ nycv'V r:,<O ~ $' ,," r:,0; fi,':5 '(}.o/ .. • • .. 0.00001 0.000001 0.0000001 ., iii " '" 1 E-08 C> o ::. 1 E-09 1 E-10 1 E-11 R>(;)O) ,\\rd-'C ",0) fv<:l ~~ ,,<;:; • Westwater Creek Dissolved Radionuclide Concentrations (uCi/ml) ,,(;) f!.-(;) ~"v'l! • • ,,(;) f!.-(;) ~'l! R>"(;) ~'C <6-" ,,(;) ~ \"'0 ,,'- ,," fv(;) rV"v'O I • U-Nat. .Th-230 .. Ra-226 ,," R> rd-rd-'C ,," ~ ~~ ,," ~ ~ ,,'l! R>""v ~~'l! 0.000001 0.0000001 ., iii u en 1 E-08 Cl o -' 1E-09 1 E-10 f?'<> ~'-~ ,*,"''0 Westwater Creek Suspended Radionuclide Concentrations (uCi/ml) -fJ() r;}rf -fJ"> ~rfJ -fJ'<> ~,,~ ,,'V -fJ'O ,*,,,<:J " r;}() ~ • U-Nat _ Th 230 .. Ra-226 I ~ ~'V f>'O ~ ,,'- "f'Oj q}{'i • White Mesa MiU-Standard Operating Procedures Book #1 I: Environmental Protection Manual, Section 2. I Date: 2/07 Revision: DUSA· I Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one):(S;it(m.lYg;;tCree~stwater Canyon Other (describe). ___ _ DATE: 1-J../() BY: 12. ~. (Sampler's initials) pH BUFFER 7.0 __ 71-' {)=--__ pH BUFFER 4.0 _--L't.!..... ",,0,--_ SPECIFIC CONDUCTIVITY __ ..... qc..C('-'-'g'--__ ----IuM..,.,H"'O""S STEAM DEPTH: pHofWATER ___________ _ COND umhos 13$, 0 • pH Units 1. 1"1 Temp ·C ______ J""-'-( -'-" ,,,,,,3'-.Jt,--_ COND Ilmhos 13 t . .3 pH units t ti Temp ·C ---,.f-2....!1..:.., .... 3_1-,--_ Conunents: ~UI'vf, TEMP _______ _ . , COND Ilmhos Z Pl. I • pH units 7 . f r Temp ·C ~.,.,.2....!.1..:.... ,,LI.+Z __ COND Ilmhos 3 It.:> pH units $".0 ( Temp·C 2/. > 7 White Mesa Mill -Standard Operating Procedures Book #11: Environmental Protection Manual, Section 2. J Date: 2107 Revision: DUSA·l Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one):Cottonwood Cre Westwater Can ther (describe), ___ _ DATE: &Z-I(; pH BUFFER 7.0 _____ _ BY: re, p. (Sampler's initials) pH BUFFER 4.0 _____ _ SPECIFIC CONDUCTIVITY ________ -"u"'M"'H.,.,O""s STEAM DEPTH: pHofWATER ___________________ _ TEMP ______ __ .. CONDurnhos COND ~rnhos pH Units pH units Temp·C Temp·C COND~rnhos CONDllmhos pH units pH units Temp·C Temp·C Comments: !t;,.-<-<a /Jta c~ ~ bJ~ II~ 'i_L White Mesa Mill -Standard Operating Procedures Book #J J: Environmental Protection Manual, Section 2.1 Date: 2107 Revision: DUSA-I Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one):Cotto;wood C~estwater Canyon Other (describe). ___ _ DATE: II/(.gd(O BY: h .! J (Sampler's initial!) pH BUFFER 7_0 _.......:...7."'--, _0 __ pH BUFFER 4.0 _-<'f...:.--"'.{J __ _ SPECIFIC CONDUCTIVITY ___ fL' ..1.'!...!S'"-___ ""uM""H"O""'s STEAM DEPTH: pHofWATER ___________ _ TEMP __________ _ COND umhos It:,.? pH Units _7 .... -'-AJ.""Lt'-'--___ _ Temp °c ....:Y::J.uo.-Sc:y'---__ COND I1mhos 71l" y .'3. pHunits " 7$ Temp °c Lt-47 Comments: I . ""/ie "!,., '<1. COND I1mhos 7$"'i.6 pH units 7. :l. 3 TempoC 4.Y, COND I1mhos 7$'6.7 pH units 7.6 '"J Temp °c '-\. '1" . ,'/."./ /., I .. l'1 ... ".. /, r.' .-> "'''' « , . , White Mesa Mill-Standard Operating Procedures Book 1111: Environmental Protection Manual, Section 2.1 0 ) Date: 2107 Revision: DUSA-t Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one):Cottonwood Creek W§st:ater C;yoii:other (describe) ___ _ !OLv-h'-W.:.-S Dy Pk-iQ b/lw (./;;1 c:icut c.v ~ pt~ DATE: /1/1 ;U.:IO ~ BY:~"'-/2./..q, (Sampled initi!llS) pH BUFFER 7.0 _____ _ pH BUFFER 4.0 _____ _ SPECIFIC CONDUCTIVITY ________ -"u"'M ... H...,O~s STEAM DEPTH: pHofWATER __________ _ TEMP ______ __ , ' COND "'urnh'"""o"'s'--___ _ COND !.l."-rnh"",,os~· __ -=-_ pH Units ______ _ pH units ______ _ Temp·C ______ _ Temp·C _____ _ COND!.l~rnh~os'__ ___ _ COND !.l~rnh""o""s,--~· _' __ pH units ______ _ pH units ______ _ Temp·C ______ _ Temp·C ______ _ Comments: II j 1/ ~!.f Ii! .)..1'tm01 '"~.~. ~ . 7f~. ,. . I~ , '" .... !/t':: ,,'.', I " /~. l.~tl ·· .\. . ).r·~~. ", "~"" •. 4 '" • ..i/It." • (. ", ~ . " ~;,.,. ". \~ .. ., 'f t, "/1i '. . .,";\ .' .' ~, . J • , . ., ",~ .• ~ .:fit. .,..,).. , ..... '\ . ""';~. .,' . .' ',' " ,. . ;'..,:, , " '. .. .'<'n' ~ ~:., " •• .. . ' .; .. / ,,,' .... I • • 1 ~ol.r. ~ ',.;a'"l ':' .. ,'" \' " '"'' :""~r)' 1 .,,\, " l' .; .' .' I; . ,.~~ :t' f' :'. ;,f t " ~ , I ". • .; ".. I .' • , " '. '. , " • I: \ ,:", , '·,·····t "1 " ~ ·~t ., ~ , .... '. '. .., . . ... . . , . , !" . , ........ , ..... • ~,;"O: ';-',. I "', ''''', <';'.' l . l ...... 11 l ',' '.': ~ ," } .f', , .-f.." ; r 1:9-, ; /' I . (l it I, , ",p . I ' .> ( (f~' . I • , ~. I " . ' ,.,& ;;," , '" A "'., r. , (' '. I ,'~ • I.; ';,1,.' f. . 'fe'" '., .. ,,. "'Y' " ; t .. r ~~. ~ J " • I ~ ~ •.• ""1&'.,,/.· , '. > '! ' " ( l' I'~.: r ,. ". '. " ,.' ~ ::",~, ~;~~: rm-EI'oERGY ,\1 )) AI l.;);' J www.energylab.com AMItfJtM £xcdttcf Si7u 1m H.len., MT 817-472-0711 • Billing., MTSOO-135-«89 • Casp", WY 881-235-0515 Gill.lt8, WY 1&&-&8&-1115 • Rapid City, SO 818-&12-1225 • ColI.g. St.tion, IX 188-&90-2218 August 19, 2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: Cl0080203 ANALYTICAL SUMMARY REPORT Project Name: 3rd Quarter Surface Water Energy Laboratories, Inc. received the following 2 samples for Denison Mines USA Corp on 8/512010 for analysis. Sample 10 Client Sample 10 Coliect Date Receive Date Matrix Test C10080203-001 Cottonwood 08/02/1013:4508/05/10 Aqueous Solids, Total Dissolved Solids, Total Suspended Cl0080203-002 Temp Blank 08/02/1000:0008/05/10 Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted lor testing. If you have any questions regarding these test results, please call. Report Approved By: cS¥~ £l llltJ.~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2010.08.1911:04:10 -06:00 Page 1 of 7 CLIENT: ¥IWW.energylab.com _ExuIIMI<fSllu ,m Denison Mines USA Corp Project: 3rd Quarter Surface Water Sample Delivery Group: C10080203 ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) • Casper, Report Date: 08/19/10 CASE NARRATIVE Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected). the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington : C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting MVW.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page MVW.energylab.com. Page 2 of 7 EN:RGY I\HU I," r UHi L :.., www.energylab.com AMIytJc:aI ExuIJHc. SIRu fIJI Helene, MT 877·472·0711 • Billinss, MT 800·735·4489 ' Cespar, WY 888·235·0515 Gillette, WY 866·686·7175 • Rapid City, SO 888·672·1225 • COli'S' Station, TJ( 888·690·2218 LABORATORY ANALYTICAL REPORT Client: Site Name: Denison Mines USA Corp 3rd Quarter Surface Water Lab 10: Cl0080203·001 Client Sample 10: Cottonwood Matrix: Aqueous Analyses PHYSICAL PROPERTIES Solids, Total Dissolved lOS@ 180 C Solids, Total Suspended TSS@ 105 C Lab 10: C 1 0080203·002 Client Sample 10: Temp Blank Matrix: Aqueous Analyses PHYSICAL PROPERTIES Temperature Report RL . Analyle reporting limit. Definitions: QCL -Quality control limit. Result Units 202 mglL 5880 mglL Result Units 3.0 Qualifiers Qualifiers RL 10 4 RL Report Date: 08/19/10 Collection Date: 08/02/1013:45 DateReceived: 08/05/10 MCL! QCL Method A2540 C A2540 D Analysis Date I By 08/09110 12:15/1r 08106110 13:51 / kre Collection Date: 08102110 DateReceived: 08/05/10 MCL! QCL Method Analysis Date I By E170.1 08/05/10 09:00 / kbh Mel -Maximum contaminant level. NO -Not detected al the reporting limit. Page 3 of 7 EN:RGY i\HOH'dCHIl ' ... www.energylab.com IM/JfJeM £xuIWt:4 SIJtu '151 H,lene, MT 817-472-0111 • Billin!., MT 800-735-4489 • Caspar, WY 888-235-0515 GIII,«" WY 866-686-7175 • Rapid City, SO 888-672-1225 • COli'!' Station, TJ( 888-690-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: 3rd Quarter Suriace Waler Analyte Count Result Method: A2540 C Sample 10: MBLK1_100809 Solids, T olal Dissolved TOS @ 180 C Method Blank ND Units mglL Sample 10: LCS1_100609 Laboratory Control Sample Solids, T alai Dissolved ToS @ 180 C 995 mg/L Sample 10: C100B0185-002AMS Sample Matrix Spike Solids, Tolal Dissolved TOS@ 180 C 2300 mg/L Sample 10: C10080185-002AMSO Sample Matrix Spike Duplicate Solids, Total Dissolved TOS@ 180 C 2300 mg/L Qualifiers: RL -Analyte reporting limit. Report Date: OB/19/10 Work Order: Cl 00B0203 RL %REC Low limit High Limit Run: BAL-U00809A 10 Run: BAL-l_100809A 10 99 90 110 Run: BAL·1 _100809A 10 101 90 110 Run: SAL·l 100809A - 10 101 90 110 NO -Not detected at the reporting limit. RPD RPDLlmit Qual Batch: 100809_1_SLDS-TDS-W 08/09/1012:13 08109110 12:13 0810911012:15 0810911012:15 0.3 10 Page 4 of7 rmJ· EN:RGY /\HOIIAI UHll', YMW.energylab.com ANlytJuIExuJIMICI S/nc. '1$2 Halena, MT 871-412·0111 • Billings, MT 800-135-4489 • Caspar, WY 888-235-0515 Gillatta, WY 866-886-1115 • Rapid City, SO 888-612-1225 • Collag. Station, TJ( 888-680-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: 3rd Quarter Surface Water Analyte Count Method: A2540 0 Result Sample 10: MBLK1_100606A Method Blank Units Solids, Total Suspended TSS@ 105 C ND mg/L Sample 10: LCS1_100806A Laboratory Control Sample Solids , Tolal Suspended TSS@ 105 C 122 mg/L Sample 10: C10080186-001ADUP Sample Duplicate Solids , Total Suspended TSS@ 105 C 474 mg/L Qualifiers: RL -Analyte reporting limit. Report Date: 08/19/10 Work Order: C10080203 RL %REC Low Limit High limit Run : BAL-U00806A 4.0 Run: BAL-U00806A 4.0 61 60 110 Run: BAL·1_100806A 4.0 NO - Not detected at the reporting limit. RPD RPDLimit Qual Batch: 100806A-SLDS·TSS·W 06/06/10 13:50 2.1 08/06/10 13:50 08/06/10 13:51 25 Page 5 of 7 EN:RGY I\IIOIU\I(,I,11 '~ ~.. www.energylab.com ~ ---,'" Helena, MT 817-472-0111 • Billings, MT 800-135-4489 . Cnp"" WI 888-235-0515 Gillette, WI 166-686-1115 . Rapid City, SO 888-612-1225 . College Slatloo, 11( 888-680-2218 Workorder Receipt Checklist Denison Mines USA Corp C10080203 Login completed by: Halley Ackerman Reviewed by: BL2000lkschroeder Reviewed Date: 8/10/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seats intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes III Yes III Yes D Yes III Yes III Yes III Yes III Yes III Yes III Yes III 3°e On Ice Yes D Yes III Date Received: 8/5/2010 Received by: tae Carrier name: FedEx No D No D No D No D No D No D No D No D No D No D No D No D Not Present D Not Present 0 Not Present 0' No VOA vials submitted 0' Not Applicable D Page 6 of7 "U '" (C (1) .... S, .... '=;t"!'CWU'!ftW-PLEASE PRINT IProvlde as much information as Dossible.l C~ny N~me:. Project Nrme'jtt WS. Permit. Etcn Sample Origin EPA/State Compliance: ,I~~II~ n1/AI~~ /S~ {),~/uHU ~n . ..("",,, t. L ~ State: IA.~ Yes l:iV'" No 0 Repo:~I~f~ ~~tj ~4.rJl cQ~,~a~eaJ "Phon~ -Hr ?7~ I Email (l:~,(~e~:i: Invoice Address:--' Invoic~_Contact & Phon.: Purchase Order: Qu(\tel8ottle Order: &' ... _~ ~. .I Special Report/Formats: :;: &lJ1l&[], '\7@{]@ 00§®ll!J~ .. Contact ELI prior to . ; ."'~ "'., o _ RUSH sample submittal ""'::f~~_'\.:~...Jo.,,<t=--t l:: 0 '" ~ _ for charges and C~r I~.l: ~lD;g~~ 0 ~ R scheduling-See c..~ O 0 B~c51 '" ~ w t:. Instruction Page OW EOD/EDTCElectronic Data) 6:;::l?l ~ I -g Roc~ptT .... p O POTWIWWTP Format· u -,g.Q.~ 0 :> U Comments: 3 . '0-" Ie:.,,,::,,: « 0 °c o State: 0 LEVELIV ~"'* 5 [§ r-~ (======'::'-----l o Other: 0 NELAC ~~r~ . «r-'5 On I,,, IbN E <p .!: .,:;: f--5 .£ 0..«1 gtc W "E Custody Seal E >1 W ro OnBottle Y N ~ V ' \I, U) ~ On Cooler C!) N ~:-::::-=-::=:-:-=-'-;:-----'----+----11 t . ~ iii H Intact ~ N SAMPLE IDENTIFICATION Collection Collection MATRIX Slgnatu.. ""N Name, Location, Interval, etc.) Date Time Match \!.J '(1IL..1' JOOA 1%· Z-I() JJ,{s-' I-fA} I X 'K ~::n--- If JlO Plo.rll ~ 3 ~ev:;'ID ~ 4 5 ~Y",m'1Oj . ~ o 7 ~ 8 ~ o , ~ . ~ " Custody nz'~::;'bY~'j f.~"i/.7(/"{/" -, 2..""'Jt..... j R_"""by ip''''} Dal""'"", s~""'"'. :~~r~ Rei",,'"hed b, ion"', D"em""" f S~ .... '"' R_ ... by ion"'}' Da.emme, /I .~""I",. S· K'C.'~DY~OO"W'Y' ~,,~~'nt" ..gJ.f:'J:""~~. _AA Igned Sample Disposal: Return 10 Clien!: Lab Disposat: %' -'5 . \tJ Q,\.)Jc:: ~ co~~~ ~ This serves as notice of this possibility. All sutrcontract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms. and links. EI\ERGY www.enelgyiab.com Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 . Rapid City, SD 888-672-1225 . College Station, TX 888-690-2218 A HUI,,>!' 1,1 • MI/ytitM rxu-. SInu 1m ANALYTICAL SUMMARY REPORT December 29, 2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding , UT 84511 Workorder No.: Cl0ll0506 Project Name: Semi-Annual Surface Water Energy Laboratories, Inc. Casper WY received the following 2 samples for Denison Mines USA Corp on 11 /12/2010 for analysis. Sample ID Client Sample to Collect Date Receive Date Matrix Test Cl 011 0506-001 Cottonwood 11 /11 /1009:3011 /12/10 Cl 011 0506-002 Temp Blank 11/11 /1000:0011 /12/10 Aqueous Sample Filtering Uranium, Dissolved Uranium, Suspended Digestion, Total Metals Gross Alpha minus Rn222 and Uranium Radium 226, Dissolved Radium 226, Suspended Thorium, Isotopic Thorium, Suspended Isotopic Solids, Total Dissolved Solids, Total Suspended Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: cS¥~ £) uJtJ.~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2010.12.29 14:44:30 -07:00 Page 1 of 12 Helena, MT 817·412·0111 • Billings, MT 800·135-4489 · Casper, WY 888·235·0515 Gillette WY 866-686·1115 • R. id Ci SD 888·612·1225 . Coli •• St.tion IX 888·69D·2218 CLIENT: Project: Denison Mines USA Corp Semi·Annual Surface Water Sample Delivery Group: Cl0ll0506 ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Report Date: 12/29/1 0 CASE NARRATIVE Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately aher collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOI USOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli·b . Energy Laboratories, Inc .. Billings, MT eli·g . Energy Laboratories, Inc .. Gillette, WY eli·h • Energy Laboratories, Inc .. Helena, MT eli·r · Energy Laboratories, Inc .. Rapid City, SD eli·t . Energy Laboratories, Inc .• College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL·DOH NELAC: E87641 , Radiochemical E871017; California: 02118CA; Oregon: WY200001 ; Utah: 3072350515; Virginia: 00057; Washington : C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC .. CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 12 EN:RGY A -,()P,\I'IJI • www.energyJab.com AIY/JIICM ExuIIrIa SIIIu ,m Helena, MT 817-412-0111 • Billings, MT 800-135-4489 • C"per, W'/ 818-235-0515 Gillette, W'/ 866-686-1115 • Rapid City, SD 888-612-1225 • College Station, 1X 881-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp Semi-Annual Surface Water Cl0ll0506-001 Client Sample 10: Cottonwood Analyses PHYSICAL PROPERTIES Solids, Total Dissolved TOS @ 180 C Solids, Total Suspended TSS @ 105 C METALS -DISSOLVED Uranium METALS-SUSPENDED Uranium RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC RADIONUCLIDES -SUSPENDED Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL . Analyle reporting limit. QCL -Quality control limit. Result 624 40 0.0077 ND 2.0 0.8 0.8 1.8 0.22 0.09 0.02 0.07 0.1 -0.005 0.11 0.19 0.2 0.2 0.2 Units mg/L mglL mglL mglL pCilL pC il L pCi/L pCilL pCilL pCi/L pCi/L pCi/L pCi/L pCilL pCilL pCilL pC ilL pCilL pCi/L MOG . Minimum detectable concentration Report Date: 12129/10 Collection Date: 11 /11 /10 09:30 DateReceived: 11 /12/10 Matrix: Aqueous MCLI Qualillers RL QCL Method Anatysls Date 1 By U U U 10 A2540 C 4 A25400 0.0003 E200.8 0.0003 E200.8 E900.1 E900.1 E900.1 E903.0 E903.0 E903.0 E907.0 E907.0 E907.0 E903.0 E903.0 E903.0 E907.0 E907.0 E907.0 Mel -Maximum contaminant level. ND -Not detected at the reporting limit. 11/12110 15:101lr 11/12110 15:3611r 12113110 20:251 sml 12109/10 01 :20 1 sml 11 /23/10 15:22 /ep 11 /23110 15:22 /ep 11 /23/10 15:22/ep 11 /24/10 01 :481 dmf 11 /24/10 01 :48 1 dmf 11 /24/1001 :48 1 dmf 11 /18/1016:01 /dmf 11 /18/10 16:011 dmf 11 /18/10 16:01 1 dmf 12102110 02:17 IIrs 12102110 02:17 I trs 12102110 02: 17 1 trs 11 /30/10 08:421 dmf 11 /30/10 08 :421 dmf 11 /30/10 08:421 dmf U -Not detected at minimum detectable concentration Page 3 of 12 EN:RGY I\'~()I , I 'II: ' WWN.energyiab.com AMI11kM __ ,m Helena, MT 877·472·0711 • Billings, MT 800·735-4489 • Casper, WY 811·235·0515 Gillette, WY 866-686·7175 . Rapid City, SD 888·672·1225 · College Station, IX 811·690·2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp Semi·Annual Surface Water Cl 011 0506·002 Client Sample 10: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl • Analyte reporting limit. Qel • Quality control limit. Result Units 3.0 Qualifiers Rl Report Date: 12/29/10 Collection Date: 11 /11 /10 DateReceived: 11 /12/10 Matrix: Aqueous MCU QCl Method Analysis Date / By Ell0.l 11/12110 09:20 / kbh Mel -Maximum contaminant level. ND . Not detected at the reporting limit. Page 4 of 12 EI'IIERGY Ah'J!., I 1,1 '0 Helena, MT 877-472-0111 • Billinis, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-&86-1115 • Rapid City, SO 888-612-1225 • Colleie Station, IX 818-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water Anatyte Count Result Units Method: A2540 C Sample 10: MBLK1_l01112 Solids, Total Dissolved TDS @ 180 C Method Blank ND mgIL Sample 10: LCS1_101112 Laboratory Control Sample Solids, Total Dissolved TDS @ 180 C 983 mg/L Sample 10: Cl0ll0505-007AMS Sample Matrix Spike Solids, Total Dissolved TDS@ 180 C 5760 mgIL Sample 10: Cl0ll0505-007AMSO Sample Matrix Spike Duplicate Solids, Total Dissolved TDS@ 180 C 5780 mglL Qualifiers: RL -Analyte reporting limit. MOe -Minimum detectable concentration Report Date: 12/29/1 0 Work Order: C 10110506 RL %REC Low Limit High Limit Run: BAL-l_l01112C 10 Run: BAL-l_l01112C 10 98 90 110 Run: BAL-l 101112C - 10 101 90 110 Run : BAL-l 101112C - 10 102 90 110 ND -Not detected at the reporting limit. RPO RPOLlmlt Quat Batch: 101112_2_SLDS-TDS-W 11112110 15 :00 11/1211015:00 11 /1211015:11 11 /1211015:11 0.3 10 Page 5 of 12 EI\ERGY I\M<lf" I Id " www.energylab.com AM/ytkM ExuIIo1a SbIu lISt Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 GiII,tte, WY 8&6-&8&-7175 • Rapid City, SD 118-&72-1225 · ColI'ge Station, IX 888-&90-2218 QAlQe Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water Analyte Count Result Method: A2540 0 Sample 10: MBLK1_ Solids, Total Suspended TSS@ 105 C Method Blank ND Units mgIL Sample 10: LCS1_ Laboratory Control Sample Solids, Total Suspended TSS@ 105 C 172 mglL Sample 10: Cl0ll0S06-001AOUP Sample Duplicate Solids, Total Suspended TSS@ 105 C 42.0 mgIL Qualifiers: AL -Analyte reporting limit. MOe -Minimum detectable concentration Report Date: 12/29/10 Work Order: Cl0ll0506 RL %REC Low Limit High Limit Aun: BAL-l _101112B 0.3 Aun: BAL-l _l01112B 4.0 85 50 110 Aun: BAL·l 101112B 4.0 ND -Not detected at the reporting limit. RPO RPOLImit Qual 4.9 Batch: A139895 11/1211015:31 11/1211015:31 11/12110 15:37 25 Page 6 of 12 EI\ERGY 1\ , JI" I fd ' www.energylab.com AMIyfIaIExu-. SIIxo lISt Helene, MT 877-472-0711 • Billing., MT 800-735-4489 • C!Sper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Siallon, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water Report Date: 12/29/10 Work Order: Cl 011 0506 Analyle Count Result Units RL %REC Low Limit High Limit Method: E200_8 Sample 10: LRB Uranium Sample 10: LFB Uranium Sample 10: Cl0ll0506-001BMS Uranium Sample 10: Cl0ll0506-001BMSO Uranium Method: E200_8 Sample 10: MB-28258 Uranium Sample 10: LCS2-28258 Uranium Sample 10: Cl0ll0614-004HMS Uranium Sample 10: Cl0110614-004HMSO Uranium Qualifiers: AL -Analyle reporting limit. MOe· Minimum detectable concentration Method Blank Run: ICPMS2-C_l01213A ND mgll l E-05 Laboratory Fortified Blank Aun: ICPMS2-C_l01213A 0.0559 mg/L 0.00030 112 85 115 Aun: ICPMS2-C -101213A Sample Matrix Spike 0.0597 mg/L 0.00030 104 70 130 Sample Matrix Spike Duplicate Aun: ICPMS2-C_l01213A 0.0620 mg/L 0.00030 109 70 130 Method Blank Aun: ICPMS4-C_l01208A ND mgll 7E-05 Laboratory Control Sample Aun: ICPMS4-C_l01208A 0.0968 mg/L 0.00030 97 85 115 Sample Matrix Spike Run: ICPMS4-C_ 101208A 0.0552 mg/L 0.00030 110 70 130 Sample Matrix Spike Duplicate Run: ICPMS4-C_l01208A 0.0547 mgll 0.00030 109 70 130 NO· Not detected at the reporting limit. RPO RPOLlmlt Qual 3.8 0.9 Balch: R140851 1211311012:38 12113110 14:11 12113/1020:30 12113/10 20:34 20 Batch: 28258 12109/10 01 :07 12109/1001 :11 12109/1001 :56 12109/10 02:00 20 Page 7 of 12 EN:RGY I\HOP,l,['JUI " Hel,na, MT 877-472-0711 • Billing', MT 800-735-4489 • Casper, WI 888-235-0515 Gillette, WI 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, rx 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water Analyte Count Result Units Method: E900.l Sample 10: MB-GA-0375 Gross Alpha minus Rn & U 3 Method Blank 3 Gross Alpha minus Rn & U Precision (±) 0.9 pCi/L pCi/L pCi/L Gross Alpha minus Rn & U MDC 0.8 Sample 10: LCS-GA-0375 Gross Alpha minus Rn & U Sample 10: Cl0ll0584-005CMS Gross Alpha minus An & U Sample 10: Cl0ll0584-005CMSO Gross Alpha minus Rn & U Qualifiers: RL -Analyte reporting limit. MOe -Minimum detectable concentration Laboratory Control Sample 32.4 pCi/L Sample Matrix Spike 25.2 pCi/L Sample Matrix Spike Duplicate 25.9 pCi/L Report Date: 12/29/10 Work Order: C 10110506 RL %REC Low Limit High Limit Run:G5000VV_l01122A Run: G5000VV_l01122A 113 70 130 Run : G5000VV_l01122A 88 70 130 Run : G5000VV_l01122A 91 70 130 NO -Not detected at the reporting limit. RPO RPOLlmlt Qual 2.7 Batch: GA-0375 11/23/10 15:22 11/23/1015:22 11 /23/1015:22 11/23/1017:11 27.9 Page 8 of 12 E"-ERGY 1\ rl If'' I !, I ' www.energylab.com _ru.-.SiIIu tm Helena, MT 817-472-0711 • BIlling., MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 866-686-7175 . Rapid City, SO 888-672-1225 . College St'lIon,1)( 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water Analyte Count Result Units Method: E903.0 Sample 10: Cl0l10614-004HMS Radium 226 Sample 10: C10110614-004HMSO Radium 226 Sample 10: LCS-28258 Radium 226 Sample 10: MB-28258 Radium 226 Radium 226 precision (±) Radium 226 MDC Method: E903.0 Sample 10: C10110468-001FMS Radium 226 Sample 10: Cl0110468-001FMSO Radium 226 Sample 10: MB-RA226-5003 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: LCS-RA226-5003 Radium 226 Qualifiers: RL -Analyte reporting limit. 3 3 MOe -Minimum detectable concentration Sample Matrix Spike 14 pCi/L Sample Matrix Spike Duplicate 15 pCi/L Laboratory Control Sample 16 pCi/L Method Blank ·0.2 pCVL O. I pCi/L 0.3 pCi/L Sample Matrix Spike 19 pCi/L Sample Matrix Spike Duplicate 18 pCi/L Method Blank 0.1 pCi/L 0.08 pCi/L 0.10 pCi/L Laboratory Control Sample 8.4 pCVL Report Date: 12/29/1 0 Work Order: Cl 011 0506 RL %REC Low Limit High Limit RPO RPOLlmit Qual Run: BERTHOLD 770·1_101122A 114 70 130 Run: BERTHOLD 770·1 101122A - 113 70 130 7.1 Run: BERTHOLD 770·1 101122A - 110 70 130 Run: BERTHOLD 770-1 101122A - Run: TENNELEC-3_101 115C 103 70 130 Run: TENNELEC-3_tDi I 15C 101 70 130 0.3 Run: TENNELEC-3_ 101 I 15C Run: TENNELEC·3_ 101 I I 5C 105 70 130 NO -Not detected at the reporting limit. Batch: 28258 11/29/10 21 :09 11129/10 21 :09 22.6 11129/10 21 :09 11/29/1021 :09 U Batch: RA226-5003 11 /24/1001:48 11 /24/1001:48 21 11 /24/1003:38 U 11 /24/1003:38 U -Not detected at minimum detectable concentration Page 9 of 12 EN:RGY AHOP)' r .~r~1 " www.energylab.com _1 __ SlnuII51 Helena. MT 871-472-0711 • Billing •• MT 800-735-4489 • Cosper. WY 888-235-0515 Gill.tt •• WY 866-686-7175 · Rapid City. SD 888-672-1225 · ColI.g. SI.lion. IX 888-690-2218 QA/QC Summary Report Prepared by Casper. WY Branch Client: Denison Mines USA Corp Project: Semi-Annual Surface Water Analyte Count Result Units Method: E907.0 Sample 10: LCS-RA-TH-ISO-1289 Thorium 230 Sample 10: Cl0ll0614-001FMS Thorium 230 Sample 10: Cl0ll0614-001FMSO Thorium 230 Sample 10: MB-RA-TH-ISO-1289 Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Method: E907.0 Sample 10: Cl0ll0614-001HMS Thorium 230 Sample 10: Cl0ll0614-001HMSO Thorium 230 Laboratory Control Sample 5.3 pCi/L Sample Matrix Spike 11 pCi/L Sample Matrix Spike Duplicate 10 pCi/L 3 Method Blank 0.03 0.05 0.08 pCi/L pCilL pCi/L Sample Matrix Spike 7.4 pCi/L Sample Matrix Spike Duplicate 12 pCi/L Report Date: 12/29/1 0 Work Order: Cl 011 0506 RL %REC Low Limit High Limit RPO RPOLlmlt Qual Run: EGG-ORTEC_l01117B 94 70 130 Run: EGG-ORTEC_l01117B 99 70 130 Run: EGG-ORTEC_l01117B 90 70 130 Run: EGG-ORTEC_l01117B Run: EGG-ORTEC_l011230 87 70 130 Run: EGG-ORTEC_l011230 135 70 130 Batch: RA·TH-ISO-1289 8.7 44 11/18/1016:01 11/18/1016:01 11/18/1016:01 42.1 11 /18/1016:01 U Batch: 28258 11 /30/10 08:42 11 /30/1008:42 47.4 S -Spike response is outside of the acceptance range for this analysis. Since the LCS, MS, and alliracer recoveries are acceptable the batch is approved. Sample 10: LCS-28258 Thorium 230 Sample 10: MB-28258 Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Qualifiers: RL -Analyte reporting limit. Laboratory Control Sample 10 pCi/L 3 Method Blank -0.1 0.1 0.2 pCi/L pCi/L pCi/L MOe -Minimum detectable concentration U -Not detected at minimum detectable concentration Run: EGG-ORTEC_l011230 109 70 130 Run: EGG-ORTEC_l011230 ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. 11 /30/1008:42 11/30/10 08:42 U Page 10 of 12 EN:RGY I\HOllr,l Of~1 ~ ~.. www.energylab.com ~ AMfytk:MExCllllnc.ShM 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, 1)( 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp C1 011 0506 Login completed by: Edith McPike Reviewed by: BL2000lkschroeder Reviewed Date: 11/18/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? Containerrremp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments; Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 3°C On Ice Yes D Yes 0 Date Received: 11/12/2010 Received by: ckw Carrier name: Fed Ex No D No D No D No D No D No D No D No D No D No D No D No D Not Present D Not Present D Not Present 0 No VOA vials submitted 0 Not Applicable D Sample filtered and preserved in the laboratory for dissolved metals and radionuclide's Page 11 of 12 'U OJ <0 CD ~ N o -~ N Chain of Custody and Analytical Request Record LAeONA rORI! .s ~,yName: \... I )~:.\o.-/ r1I,~F<-S. I RePOrt Mail I<uur=, ~o, I,~x gu1 'I5/hll)I:"~ lA-I ~'-In I Invoice Address: I . <;.;; ~I/\ 2: PLEASE PRINT (Provide a~mucllinformation as Project Name. PWS, Perrillt, Etc. Sc,,,,,,: Ar..'NJ. \ • ...,-tw--"-rAt.LA Phone/Fax: Contact Name: 11 I ~/'.I 1./.11// kf--Y. I & Phone: .~ ... 1.1 3: Origin ---State: tA I Email: r-Ull,.illdse Order: Page _1_ of -L 11 ...... i:tllVt:. Yes G--'" No 0 ".,"",",: (F't'/f Print) rZ~-v LLj~_ --nllniplRn"l~ -Order: ~ I ~\'7@[]~ ~~~@,@ Special Report/Formats: o ~ , ... 1 ~.'~t:'.ct ELI prior to I<U<>M sample submittal for charges and "leaf. ...k' ~O(l)~ :!!al;g OIl;; 'C: ->S~· ~ ~CI)", 1& ~ o~= ~ C'l ~ U>oo .E -«~cDl~ ~ o ··Q)c ·t: ......: ~8..roOO ." .o~riij , E~~.~ v ~Ci<IOlO .::: E ~I ~ ~ ;t ~~S-AM~PL~E~I=D=E~NT=I=FI=C~AT=I=O~N~'-~~~'-Co~II~ec~ti~On~-M-A-T-R-'-X-cf (Name. Location. Interval, etc. Time Dow o POTWNifWTP o State: ___ _ o Other: ___ _ o EOO/EOT(Electronic Data) Format:'::-:-___ _ o LEVEL IV o NELAC o :;: UJ t:. ::c 'C () § « e I-'" I-E « ~ w 'E UJ '" (f) -g c7l R I scheduling -See 'Instruction Page u • Comments: 5 H -o/kN'we&i I' [i ' ~~ ~~/L 1 /(!l2aol (rz~a 1.2-0 IX I KI XiX fX I Xl I I I I I I I CoorIer .... ~,.,. C);''l-I KtK;8lpt 19IT1p -. ~ °c I On \CO, Sear OnBottle On Coole< (YN ~~ -I I:' -I I I I Ll± II I I I I Ii I 5 '= 6 7 8 • '0 Wt2#'t?J"t1? , I Custody Record ~~~~~&-~~~~~~~~~~ Received by (prili): pO")' -'." Signature: Ml:'ST bef-----------------!7'-:....--'-_.n,,,,e, Signed Sam e Dis os.1: Return to Client: Lab Disposal: D In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to ot ified laboratories in order to complete the analysis requested. This serves as notice of this possibility, All sul>-contract data will be clearly notated on your analytical report. Vrsit our web site at www.energylab.com for additional information, downloadable fee schedule, forms. and links. ATTACHMENT I SOIL SAMPLE GRAPHS, DATA TABLE, LABORATORY RESULTS AND QAlQC + OJ I .,: ~ + OJ I .,: '" t OJ I .,: W + OJ I .,: ... + OJ I .,: en + OJ I .,: Ol o o en ~ ~ a, '" '" en w Jul-98 ~,t I " " Oct-98 Jan-99 Apr-99 Jul-99 Oct-99 Jan-OO Apr-OO Jul-OO Oct-DO Jan-01 Apr-01 Jul-01 Oct-01 Jan-02 Apr-02 Jul-02 Oct-02 Jan-03 Apr-03 Jul-03 Oct-03 Jan-04 Apr-04 Jul-04 Oct-04 Jan-05 Apr-05 Jul-05 Oct-05 Jan-06 Apr-06 Jul-06 Oct-06 Jan-O? Apr-O? Jul-O? Oct-O? Jan-08 Apr-08 Jul-08 Oct-08 Jan-09 Apr-09 Jul-09 Oct-09 Jan-10 Apr-10 Jul-10 1 .." "+ L w a, ;;0 \II el- I: 3 , N N Ol (') o :::I n ID :::I .. Cl e-o :::I VI :::I C/I 2_ -'0 (') :::.: CD ~ a ~ '" ~ ... a en ~ a. '" a. '" en ... a. JUI-98 Oct-98 Jan-99 Apr-99 - Jul-99 Oct-99 Jan-OO Apr-OO Jul-OO Oct-OO Jan-01 Apr-01 Jul-01 Oct-01 Jan-02 C + iil Apr-02 :::I OJ Jul-02 c: I 3 1: Oct-02 • Jan-03 Z III + Apr-03 r> Jul-03 C') OJ 0 I Oct-03 :::I -;:: Jan-04 n (1) '" :::I Apr-04 .. + ., Jul-04 III ~ OJ Oct-04 0 :::I I Jan-05 -;:: fII w Apr-05 :::I + Jul-05 en Oct-05 2. ~ OJ Jan-06 I "tl -;:: Apr-06 C') " ::.: Jul-06 CQ ~ + Oct-06 Jan-O? OJ I Apr-O? -;:: Jul-O? '" + Oct-O? Jan-08 OJ Apr-08 I Jul-08 -;:: 0> Oct-08 Jan-09 Apr-09 Jul-09 Oct-09 - Jan-10 Apr-10 Jul-10 BHY-I Dale Ra-V-Nat 226 917180 0.650 0.420 9/8/81 0.400 1.800 12/3/81 0.790 0.770 6/30/82 0.423 0.384 5/5/83 0.471 0.410 6/4/84 0.713 0.866 10/12/8 2.960 0.886 4 8/28/85 1.630 0.800 811 /86 0.369 0.654 8/17/87 0.600 0.800 8/28/88 1.500 1.600 8/25/8 8 1.200 1.600 811 /90 2.900 5.800 8/5/91 3.900 8.800 8/13/92 1.200 2.200 8/lJ/93 2.000 1.700 8/3/94 1.000 1.600 8/28/95 2.8 10 4.700 8/lJ/96 1.700 2.150 8/1/97 0.540 0.3 10 7/1/98 1.600 3.050 8/24/99 2.270 1.740 12/1100 l.510 1.210 8123/0 I 1.000 1.000 8/1102 1.300 1.350 8/5/03 0.800 0.990 8/9/04 0.600 0.610 8/3/05 0.900 0.960 817106 0.700 0.760 8/8/07 1.100 2.370 8/20/08 0.900 1.230 8/10109 0.800 0.880 8/2/10 1.3 1.09 *Data not available. WHITE MESA MILL Soil Sampling Results (V ALVES) x 10-3 uCi/kg BHV-2 BHV-3 BHV-4 Ra-U-Nat Ra-V-Nat Ra-V-Nat 226 226 226 0.340 0.420 0.420 0.420 0.4 10 12.194 0.300 0.600 0.300 0.600 0.200 3.000 0.440 0.560 0.890 0.420 0.750 0.630 0.412 0.180 0.265 0.207 0.478 0.260 0.569 0.550 0.46 1 0.340 0.643 0.340 0.618 0.683 0.489 0.471 0.124 0.324 2.330 0.069 2.880 0.721 3.490 0.804 2.190 0.424 2.270 0.424 4.330 0.294 0.466 0.866 0.382 0.694 0.396 0.826 1.500 0.900 0.800 0.600 1.200 0.700 1.300 0.700 0.600 0.900 1.000 1.300 1.100 3.000 0.800 1.000 1.100 1.400 1.000 1.400 0.800 1.400 1.800 1.300 1.700 2.600 2.600 5.700 1.800 2.600 0.900 1.400 0.800 1.200 0.900 0.900 1.400 1.700 1.100 1.900 0.800 1.600 0.700 0.800 0.700 0.900 0.700 1.100 0.680 0.200 0.880 0.650 0.580 0.240 0.600 0.460 0.300 0.210 0.500 0.520 0.560 0.160 0.410 0.270 0.410 0.260 0.700 0.580 0.500 0.450 1.000 1.190 0.780 0.840 0.530 0.420 0.840 0.770 0.810 0.530 * • 0.830 1.220 0.600 0.300 0.400 0.300 0.900 1.000 0.900 0.524 0.500 0.297 1.200 1.490 0.600 0.790 0.500 0.330 0.600 0.4300 0.400 0.250 0.400 0.220 0.600 0.5100 0.700 0.340 0.600 0.270 0.600 0.3800 0.440 0.250 0.410 0.250 0.520 0.480 0.700 0.530 0.200 0.550 0.500 0.740 0.300 0.430 0.600 0.980 0.500 0.790 0.700 0.540 0.700 1.080 0.800 0.610 1.0 1.49 0.8 0.62 1.3 1.69 BHV-5 BHV-6 Ra-V-Nat Ra-V-Nat 226 226 0.230 14.89 I - 0.300 0.600 - 0.550 0.420 - 0.449 0.2 16 - 0.147 0.140 - 0.132 0.3 10 -- 2.550 0.81 7 -- 1.280 0.577 - - 0.728 0.836 - - 1.500 1.300 - - 3.800 5.000 -- 2.900 5.700 -- 3.700 3.200 - - 2.500 4.400 -- 1.100 1.800 - - 4.800 3.500 -- 3.000 3.800 -- 2.800 1.600 - - 1.900 2.010 - 1.700 1.500 - 3.000 2.760 -- 3.270 3.150 - - 2.810 3.250 -- 1.200 1.1 00 - 2.400 2.8 10 60.00 0.550 0.280 0.420 0.600 0.530 1.000 1.400 0.900 1.400 0.700 0.410 1.000 1.200 1.400 1.300 0.780 0.650 1.100 1.450 0.800 0.930 0.800 1.330 0.500 0.670 2.600 2.980 0.500 0.810 1.7 1.69 0.8 0.87 EN:RGY "\1 )j. d (I, .~ www.energylab.com AMIftIa/~.Qa 1m H.len., MT 817-472·0711 • Billing., MT 800·735·«89 · ClSpar, 'If1 888·235·0515 Gill.tt., 'If1 1&6·686·7175 • R.pid City, SO 888·672·1225 • ColI.g. St,tion, IX 888·690·2218 Seplember 17, 2010 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: Cl0080251 ANALYTICAL SUMMARY REPORT Project Name: Annual Soil Samples Energy Laboratories , Inc. received the following 6 samples for Denison Mines USA Corp on 8/6/2010 for analys is. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test Cl 0080251·001 BHV·l 08/02/1010:4008/06/10 Solid Uranium, Total Digestion For RadioChemistry Radium 226 Cl0080251·002 BHV·2 08/02/10 10:55 08/06/10 Solid Same As Above Cl0080251·003 BHV·3 Black Mesa 08/02/10 11 :20 08/06/10 Solid Same As Above Cl0080251·004 BHV·4 08/02/10 13:12 08/06/10 Solid Same As Above Cl0080251·005 BHV·5 08/02/10 12:45 08/06/10 Solid Same As Above Cl 0080251·006 BHV·6 08/02/10 12:55 08/06/10 Solid Same As Above This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate on ly to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Report Approved By: ~~£l uJrJ.~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2010.09.1717:34:00 ·06:00 Page 1 of 12 WNW.energylab.com AIu/JtiCII ExuIJnl:t SIRe. 1m Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillott. WY 866-686-7175 ' Ra Id CI so 888-672-1225 ' Coli •• Station TX 888-690-2218 CLIENT: Project: Denison Mines USA Corp Annual Soil Samples Sample Delivery Group: Cl0080251 ORIGINAL SAMPLE SUBMITIAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Report Date: 09/17/10 CASE NARRATIVE Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated . ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for aJi seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. It so, ENERGY LABORATORIES wilt utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station , TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E8764 t , Radiochemical E87t 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com . Page 2 of 12 E~RGY j\\JOP/I.!GIlIl <J www.energylab.com _1 __ ,1St Helena, MT 817-412-0111 • Billings, MT 800-135-448S • Casper, WI 888-235-0515 Gille"., WI 866-686-7175 • Rapid City, SD 888-612-1225 • ColI.g. Siallon, TJl888-6S0-2218 LABORATORY ANALYTICAL REPORT Client: Project: LablD: Denison Mines USA Gorp Annual Soil Samples Cl0080251-001 Client Sample ID: BHV-l Analyses METALS-TOTAL Uranium RADIONUCLIDES -TOTAL Radium 226 Radium 226 precision (±) Radium 226 MOe Report Definitions: RL • Analyte reporting limit. QCL -Quality controllimil. Result 1.61 1.3 0.2 0.09 Units mglkg-dry pCi/g-dry pCi/g-dry pCi/g-dry MDe -Minimum detectable concentration Qualifiers RL 0.02 Report Date: 09/17/10 Collection Date: 08/02/10 10:40 DaleReceived: 08/06/10 Matrix: Solid MCU QCL Method Analysis Date I By SW6020 08/25/1022:351 sml E903.0 08/25/1009:18 /1rs E903.0 08/25/1009:18/1rs E903.0 08/25/1009:18/1rs MeL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 12 EN:RGY i\1 )1' <I( "I ' www.energylab.com ___ '151 Helena, MT 817-472-11711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 GIII.tte, WY 866-686-7115 • Rapid City, SO 888-672-1225 • College Siallon, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: Denison Mines USA Corp Annual Soil Samples Lab 10: C 1 0080251-002 Client Sample 10: BHV-2 Analyses METALS -TOTAL Uranium RAD10NUCLIDES -TOTAL Radium 226 Radium 226 precision (±) Radium 226 MOe Report Definitions: RL • Analyte reporting limit. QCL • Quality control limit. Result 2.20 1 0.2 0.09 Units mg/kg-dry pCi/g-dry pCi/g-dry pCi/g·dry MOe -Minimum detectable concentration Qualifiers Rl 0.02 Report Date: 09/17/10 Collection Date: 08/02/10 10:55 DateReceived: 08/06/10 Matrix: Solid MCU eCl Method Analysis Date I By SW6020 08/25/10 22:431 sml E903.0 08125/10 09:18 Itrs E903.0 08125/10 09:18 Itrs E903.0 08125/10 09:18 Itrs Mel -Maximum contaminanllevel. NO -Not detected althe reporting limit. Page 4 of 12 EN:RGY ,\ )1,," (II , lWtW.energylab.com ~ ExuIIMtct sac. ,m Helena, lIT 811-472-0711 • 8111ing., MT 800-735-4489 • Cnper, WY 888-235-0515 G111.H., WY 866-886-7175 • Rapid City, SO 888-672-1225 • ColI.g. Slat1on, TJ1888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab tD: Denison Mines USA Corp Annual Soil Samples Cl0080251-003 Client Sample ID: BHV-3 Black Mesa Analyses Result METALS -TOTAL Uranium RAD10NUCLIDES -TOTAL Radium 226 Radium 226 precision (±) Radium 226 MOe Report Definitions: RL . Analyle reporting limit. aCL -Quality control limit. 0.92 0.8 0.1 0.1 MOe -Minimum delectable concentration Units mglkg-dry pei/g-dry pei/g-dry pei/g·dry Qualifiers Rl 0.02 Report Date: 09/17/10 Collection Date: 08/02/1011 :20 DateReceived: 08/06/10 Matrix: Solid Mew ael Method Analysis Date I By SW6020 08/25/1022:47 / sml E903.0 08/2511009:18 /lrs E903.0 08/25/1009:18 /lrs E903.0 08/25/10 09:18 / Irs MeL -Maximum contaminanllevel. NO -Not detected althe reporting limit. Page 5 of 12 EN:RGY 1I.110HAIOHII " www.energytab.com _fxuIIHuSiRuII51 Helena, MT 811-412-0111 • Billings, MT 800-135-4489 • Caspar, WY 888-235-0515 Gillette, WY 866-&86-1115 • Rapid City, SO 888-612-1225 • Collega Siallon, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project : Lab 10: Denison Mines USA Corp Annual Soil Samples C10080251-004 Client Sample 10: BHV-4 Analyses Result METALS -TOTAL Uranium RADIONUCLIDES -TOTAL Radium 226 Radium 226 precision (±) Radium 226 MOe Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. 2.50 1.3 0.2 0.1 MOe - Minimum delectable concentration Units mglkg-dry pei/g-dry pei/g-dry pei/g-dry Qualifiers RL 0.02 Report Date: 09/17/10 Collection Date: 08/02/1013:12 DateReceived: 08/06/10 Matrix: Solid MCU aCL Method Analysis Date I By SW6020 08/25/1022:51 I sml E903.0 08/25/1009:18 /1rs E903.0 08/25/10 09:18 I Irs E903.0 08/25/10 09:18 I Irs Mel -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 12 EN:RGY /\' :)IU' I {I" " ~.energylab.com AIuIytDIlxcIIIncI SiIIu ,m Helena, NT 817-412-0111 • Billin!_, MI 800-135-4489 • C"per, WY 888-235-0515 GIII.tt., WY 866-186-1115 • Rapid City, SO 888-612-1225 • Colle!. Siallon, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab ID: Denison Mines USA Corp Annual Soil Samples Cl0060251-005 Client Sample ID: BHV-5 Analyses Result METALS -TOTAL Uranium RADIONUCLIDES -TOTAL Radium 226 Radium 226 precision (±) Radium 226 MDe Report Definitions: RL • Analyte reporting limit. aCL . Quality control limit. 2.50 1.7 0.2 0.1 MDe • Minimum delectable concentration Units mglkg·dry pCi/g·dry pCi/g-dry pCi/g-dry Qualifiers Rl 0.02 Report Date: 09/17/10 Collection Date: 06/02/101 2:45 DateReceived: 06/06/10 Matrix: Solid MCU aCl Method Analysis Date I By SW6020 08/25/10 22:55 1 sml E903.0 08125/10 09: 181 Irs E903.0 08/25/1009:181 Irs E903.0 08/25/1009:181 trs Mel -Maximum contaminant level. ND -Not detected at the reporting limit. Page 7 of 12 EN:RGY I\l~Or<AIOIlIl .~ www.energytab.com AIu/ytk:IllxuIIHct SiJru 1m Helena, lIT 817-472-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 866-&86-1115 • Rapid City, SO 888-672-1225 • ColI.g. Sialion, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Client: Project: Lab 10: Denison Mines USA Corp Annual Soil Samples C10080251-006 Client Sample 10: BHV-6 Analyses METALS -TOTAL Uranium RADIONUCLIDES -TOTAL Radium 226 Radium 226 precision (±) Radium 226 MOe Report Definitions: RL . Analyte reporting limit. aCL -Quality con\rollimit. Result 1.28 0.8 0.1 0.09 Units mg/kg·dry pei/g·dry pei/g·dry pei/g-dry MOC . Minimum delectable concentration Qualifiers RL 0.02 Report Date: 09/17/10 Coliection Date: 08/02/10 12:55 DateReceived: 08/06/10 Matrix: Solid MCU QCL Method Analysis Date I By SW6020 08/25/10 22:591 sml E903.0 08/25/1009:18 1 Irs E903.0 08/25/1009:181 Irs E903.0 08/25/1009:181 Irs Mel -Maximum contaminant level. NO . Not detected at the reporting limit. Page 8 of 12 EN:RGY " r i " I" ' www.energylab.com MMybI £xuIIHct sac. 'Ill Heleno, NT 877-472-0711 • Billing., MT 800-735-4488 • Cnp .. , WY 888-235-0515 Gillette, WY 866-&86-7175 • Rapid City, SO 888-672-1225 • Colloge St.tion, IX 888-680-2218 QA/QC Summary Report Cllen1: Denison Mines USA Corp Project: Annual Soil Samples Analyte Count Result Units Method: E903.0 Sam pte 10: Cl0080309-004CMS Radium 226 Sample to: Cl0080309-004CMSO Radium 226 Sample tD: LCS-27037 Radium 226 Sample Matrix Spike 9.9 pCilg-dry Sample Matrix Spike Duplicate 9.4 pCilg-dry Laboratory Control Sample 1.9 pCilg·dry Report Dale: 09117110 Work Order: C 1 0080251 RL %REC Low Limit High limit RPO RPOLlmlt Quat Run: 118 Run: 108 Run: 131 BERTHOLD 770-2_100819A 70 130 BERTHOLD 770-2_100819A 70 130 5.3 BERTHOLD 770-2 100819A - 70 130 Batch: 27037 08125110 10:48 08125110 10:48 24.5 08125110 10:48 S -Les response is outside of the acceptance range for this analysis. Since the MS, MS, and MSD are acceptable the balch is approved. Sample 10: MB-27037 Radium 226 Radium 226 precision (±) Radium 226 MDC Qualifiers: RL -Analyte reporting limit. 3 Method Blank -0.0003 pCilg-dry 0.0002 pCilg-dry 0.0004 pCilg-dry MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration Run: BERTHOLD 770-2_100819A 08125/10 10:48 U ND -Not detected at the reporting limit. S . Spike recovery outside of advisory limits. Page 9 of 12 EN:RGY At ) I , "I' ' www.energylab.com Alulytal buIIn&t SIJtu ,m Hel.na, NT 877-412-0711 • Bimngs, MT 800-735-«89 • Cuper, WY 888-235-0515 Gilletle, WY 866-&86-7175 • Rapid City, SO 888-672-1225 • College Station, TJ( 888-690-2218 QA/QC Summary Report Client: Denison Mines USA Corp Project: Annual Soil Samples Analyte Count Result Units Method: SW6020 Sample to: MB-27037 Uranium Sample 10: LCS2-27037 Uranium Sample 10: Cl00B0309-004CMS Uranium Sample 10: Cl00B0309-004CMSO Uranium Qualifiers: RL -Analyte reporting limit. MOe -Minimum detectable concentration Method Blank 0.0001 mg/kg·dry Laboratory Control Sample 5.51 mg/kg-dry Sample Matrix Spike 7.77 mglkg-dry Sample Matrix Spike Duplicate 7.91 mglkg·dry Report Date: 09/17/10 Work Order: Cl0080251 RL %REC Low Limit High Limit RPO RPDLimit Qual Batch: 27037 Run: ICPMS4-C_l00825A OB/2511 0 22:06 4E-05 Run: ICPMS4-C_'00B25A 08/2511 0 22: 1 0 0.D15 110 75 125 Run: ICPMS4-C_l00825A 08/2511 0 23:24 0.015 118 75 125 Run : ICPMS4-C_l00825A 08/25/1 023:28 0.015 120 75 125 1.7 20 NO -Not detected at the reporting limit. Page 10 of 12 EI\ERGY ,I\IIOHJ\'<,'I'll " ~.. 'ItWW.energylab.com ~ AIII/JfkIIExuIIHuSlnu lIst Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-&86-71 75 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp II II 1111111111 11111 ~III I I C10080251 Login completed by: Halley Ackerman Reviewed by: BL2000lkschroeder Reviewed Date: 8/10/2010 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/botUe? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water· VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes III Yes III Yes D Yes III Yes III Yes III Yes III Yes III Yes III Yes III 23'C Yes D Yes D Date Received : 8/6/2010 Received by: ckw No D No D No D No D No D No D No D No D No D No D No D No D Carrier name: 2nd Day Air Not Present 0 Not Present 0 Not Present 0" No VOA vials submitted 0" Not Applicable III Page 110112 -u '" (Q <D '" 2- ~ '" 'ftwue·u-lll!.I7' PLEASE PRINT (Provide as much information as DossibJe.1 -~ Ccxnj5;:; ~o'" rY1 ;I'IE:S projt1~a~:_T~~:~/' EtSa ~D / ,~~ Sample Origin EPNState Compliance: State: u.-r-Yes [iJ..-No 0 Report Mail.Add:~~ 8~9 Contact Name: PhoneiFax: ' Email: Sampler: (Please Print) J2\1AAl [) I Paf:.Jr';{';"";' IA7" PI( SII , t.'7Y'7?? I --r -IL /1:Je... Invo;ce Address: -I Invoice Contact & Phone: Purchase Order: Quote/Bottle brder: ~ ..-J ~A A' ~.-..L Special Report/Formats: ~ 'l7®[]@ rn@:@(lD~@) .. Contact ELI prior to I 'hlppod by, , ;;; tM~ U>R I Cl li; RUSH sample subm~tal ~OCl).J:: ~ for charges and COoler ID(s): il!mgC5! li; 0 « R scheduling -See C~ ._> 0 >-00 W !::. Instruction Page ~<I)~m;;; o DW 0 EDD/EDT(ElectrOl1ic Dala) o~:a~ C) I "0 RK8iptTemp () c: Comments: o POTWfWWTP Format: u~cnJ.Q ~ " U ?-2> '0 .... COI r::: <I: Ie °c o State: 0 LEVEL IV •• ClI c:'-I-'" .... ~cagc l-E o Other: 0 NELAC ~0!I ", ' <I: " On Ice: v<E,) ~.9:!:;ZI~~ 1-;:; . ~ f--S Z c. ., W E Custody Seal ~ >1 W '" Co ..... ~: ~ (/) '0 <I) ~ c: Co Coolo< '" ~ ii5 H Intact SAMPLE IDENTIFICATION Collection Collection f"::::: (Name. Location,lnterval, etc.) Date Time MATRIX Signature C!>N Match ~RIW-I Ix-.?/h ,a~ D I-oS X )( b 'RlI-t/ -?. 1 ~.7-/{) InXS-J -S X )( ]I I 151W -3 B/""k meSA. Isr-7.,O " to /-.s y.. )l ft..IIV -4 :i". z ·/{j 1312... /-$ ~ )C ,1')\ 'SHv',r ;r·7 'Ill In'iS' "-5 ., x ~ ,g/l-v-h I~·Z ·ID IltsS-1-.$ I)' ~ ~ 1 ~ 8 ~ a 9 00 ~ " IA ~ Custody ~:"b:(P:tL o"omme I'fDO ---,-2~' ~~ Received by (print): DatefTime: Signature: .r X·4./D ::.z. oj Record RelinqUlhed by (pnnt~ Ua!eI lme: ;:j' Sigrt lure: ..... Received by (print): OatelTime: Signature: MUST be Signed , .'<"r''f~ II A i"r.:'1o ~\:5 Signa ure: Sample Disposal: Return to Client: Lab Disoosal: In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other ~~Iaboratories in order to complete the analysis requested. This serves as notice of this possibility_ All sub-contract data will be clearly n on your analytical report. www.en~gi1ab.com