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HomeMy WebLinkAboutDRC-2015-002544 - 0901a06880530e7bENERGYFUELS DRC-2015-002544 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www.energvfuels.com May 20, 2015 Sent VIA OVERNIGHT DELIVERY Mr. Rusty Lundberg Division of Radiation Control Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144850 Salt Lake City, UT 84114-4820 Re: Transmittal of 1st Quarter 2015 Nitrate Monitoring Report Stipulation and Consent Order Docket Number UGW12-04 White Mesa Uranium Mill Dear Mr. Lundberg: Enclosed are two copies of the White Mesa Uranium Mill Nitrate Monitoring Report for the 1st Quarter of 2015 as required by the Stipulation and Consent Order Docket Number UGW12-04, as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours very truly, - ENERGY FUELS RESOURCES (USA) INC. Kathy Weinel Quality Assurance Manager cc: David C. Frydenlund Dan Hillsten Harold R. Roberts David E. Turk Scott Bakken White Mesa U rani urn Mill Nitrate Monitoring Report State of Utah Stipulated Consent Agreement, December 2014 Docket No. UGW12-04 1st Quarter (January through March) 2015 Prepared by: Energy Fuels Resources (USA) Inc. 225 Union Boulevard, Suite 600 Lakewood, CO 80228 May 20,2015 TABLE OF CONTENTS 1.0 INTRODUCTION ................................................................................................. 1 2.0 GROUNDWATER NITRATE MONITORING ................................................ ! 2.1 Samples and Measurements Taken During the Quarter ..................................... 1 2.1.1 Nitrate Monitoring ...................................................................................... 2 2.1.2 Parameters Analyzed ................ -................................................................... 3 2.1.3 Groundwater Head and Level Monitoring .................................................. 3 2.2 Sampling Methodology and Equipment and Decontamination Procedures ....... 4 2.2.1 Well Purging, Sampling and Depth to Groundwater .................................. 4 2.2.2 Piezometer Sampling .................................................................................. 5 2.3 Field Data ............................................................................................................ 5 2.4 Depth to Groundwater Data and Water Table Contour Map .............................. 5 2.5 Laboratory Results .............................................................................................. 5 2.5.1 Copy of Laboratory Results ........................................................................ 5 2.5.2 Regulatory Framework ............................................................................... 6 3.0 QUALITY ASSURANCE AND DATA VALIDATION ................................... 6 3.1 Field QC Samples ............................................................................................... 6 3.2 Adherence to Mill Sampling SOPs ..................................................................... 7 3.3 Analyte Completeness Review ............................................................................ 7 3.4 Data Validation ................................................................................................... 7 3.4.1 Field Data QA/QC Evaluation .................................................................... 7 3.4.2 Holding Time Evaluation ............................................................................ 8 3.4.3 Analytical Method Checklist ...................................................................... 8 3.4.4 Reporting Limit Evaluation ........................................................................ 9 3.4.5 QA/QC Evaluation for Sample Duplicates ................................................. 9 3.4.6 Other Laboratory QA/QC ........................................................................... 9 3.4.7 Receipt Temperature Evaluation ............................................................... 10 3.4.8 Rinsate Check ........................................................................................... 10 4.0 INTERPRETATION OF DATA ....................................................................... 10 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions ........... 10 4.1.1 Current Site Groundwater Contour Map ................................................... 10 4.1.2 Comparison of Current Groundwater Contour Map to Groundwater Contour Map for Previous Quarter .................................................................................. 14 4.1.3 Hydrographs .............................................................................................. 15 4.1.4 Depth to Groundwater Measured and Groundwater Elevation ................. 15 4.2 Effectiveness of Hydraulic Containment and Capture ...................................... 15 4.2.1 Hydraulic Containment and Control.. ....................................................... 15 4.2.2 Current Nitrate and Chloride Isoconcentration Maps ............................... 18 4.2.3 Comparison of Areal Extent ............................................................................ 18 4.2.4 Nitrate and Chloride Concentration Trend Data and Graphs .................... 19 4.2.5 Interpretation of Analytical Data .............................................................. 19 4.3 Estimation of Pumped Nitrate Mass and Residual Nitrate Mass within the Plume .......................................................................................................................... 21 5.0 LONG TERM PUMP TEST AT TWN-02, TW4-22, TW4-24, and TW4-25 OPERATIONS REPORT .................................................................................. 22 5.1 Introduction .......... , ............................................................................................ 22 5.2 Pumping Well Data Collection ......................................................................... 23 5.3 Water Level Measurements .............................................................................. 23 5.4 Pumping Rates and Volumes ............................................................................ 23 5.4.1 TW4-19 ............................................................................................................ 24 5.4.2 TW4-02 ............................................................................................................. 24 6.0 CORRECTIVE ACTION REPORT ................................................................. 25 6.1 Assessment of Previous Quarter's Corrective Actions ..................................... 25 7.0 CONCLUSIONS AND RECOMMENDATIONS ............................................ 25 8.0 ELECTRONIC DATA FILES AND FORMAT .............................................. 28 9.0 SIGNATURE AND CERTIFICATION ........................................................... 29 Table 1 Table 2 Table 3 Table 4 Table 5 Table 6 Table 7 Table 8 LIST OF TABLES Summary of Well Sampling and Constituents for the Period Nitrate Mass Removal Per Well Per Quarter Nitrate Well Pumping Rates and Volumes Qumterly Calculation of Nitrate mass Removed and Total Volume ofWater Pumped Nitrate Data Over Time for MW-30, MW-31, MW-5, and MW-11 Slug Test Results Pre-Pumping Saturated Thickness Pre-Pumping Hydraulic Gradients and Flow Calculations 11 INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and Field Data Worksheets Tab C Kriged Current Quarter Groundwater Contour Map and Weekly, Monthly and Quarterly Depth to Water Data Tab D Kriged Previous Quarter Groundwater Contour Map Tab E Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells Tab F Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Tab G Laboratory Analytical Reports Tab H Quality Assurance and Data Validation Tables H-1 Field Data QA/QC Evaluation H-2 Holding Time Evaluation H-3 Analytical Method Check H-4 Reporting Limit Evaluation H-5 QAJQC Evaluation for Sample Duplicates H-6 QC Control limits for Analysis and Blanks H-7 Receipt Temperature Evaluation H-8 Rinsate Evaluation Tab I Kriged Current Quarter Nitrate and Chloride Isoconcentration Maps Tab J Analyte Concentration Data Over Time Tab K Nitrate and Chloride Concentration Trend Graphs Tab L CSV Transmittal Letter Tab M Residual Mass Estimate Analysis Figures and Tables AWAL CA CAP CIR DIFB DRC EFRI ft amsl GWDP LCS MS MSD QA QAP QC RPD sco SOPs UDEQ voc ACRONYM LIST American West Analytical Laboratory Consent Agreement Corrective Action Plan Contamination Investigation Report Deionized Field Blanks Utah Division of Radiation Control Energy Fuels Resources (USA) Inc. feet above mean sea level Groundwater Discharge Permit Laboratory Control Spike Matrix Spike Matrix Spike Duplicate Quality Assurance Groundwater Monitoring Quality Assurance Plan Quality Control Relative Percent Difference Stipulated Consent Order Standard Operating Procedures Utah Department of Environmental Quality Volatile Organic Compounds iv 1.0 INTRODUCTION The Utah Department of Environmental Quality ("UDEQ") Division of Radiation Control ("DRC") noted in a Request dated September 30, 2008 (the "Request"), for a Voluntary Plan and Schedule to Investigate and Remediate Nitrate Contamination at the White Mesa Uranium Mill (the "Mill") (the "Plan"), that nitrate levels have exceeded the State water quality standard of 10 mg/L in certain monitoring wells. As a result of the Request, Energy Fuels Resources (USA) Inc. ("EFRI") entered into a Stipulated Consent Agreement with the Utah Water Quality Board in January 2009 which directed the preparation of a Nitrate Contamination Investigation Report ("CIR"). A subsequent letter dated December 1, 2009, among other things, recommended that EFRI also address elevated chloride concentrations in the CIR. The Stipulated Consent Agreement was amended in August 2011. Under the amended Consent Agreement ("CA"), EFRI submitted a Corrective Action Plan ("CAP"), pursuant to the requirements of the Utah Groundwater Quality Protection Rules [UAC R317-6-6.15(C-E)] on November 29, 2011 and revised versions of the CAP on February 27, 2012 and May 7, 2012. On December 12, 2012, DRC signed the Stipulation and Consent Order ("SCO"), Docket Number UGW12-04, which approved the EFRI CAP, dated May 7, 2012. The SCO ordered EFRI to fully implement all elements of the May 7, 2012 CAP. Based on the schedule included in the CAP and as delineated and approved by the SCO, the activities associated with the implementation of the CAP began in January 2013. The reporting requirements specified in the CAP and SCO are included in this quarterly nitrate report. This is the Quarterly Nitrate Monitoring Report, as required under the SCO, State of Utah Docket No. UGW12-04 for the first quarter of 2015. This report meets the requirements of the SCO, State of UDEQ Docket No. UGW12-04 and is the document which covers nitrate corrective action and monitoring activities during the first quarter of 2015. 2.0 GROUNDWATER NITRATE MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of all groundwater monitoring wells, piezometers, existing wells, temporary chloroform contaminant investigation wells and temporary nitrate investigation wells is attached under Tab A. Nitrate samples and measurements taken during this reporting period are discussed in the remainder of this section. 1 2.1.1 Nitrate Monitoring Quarterly sampling for nitrate monitoring parameters was performed in the following wells: TWN-1 TWN-2 TWN-3 TWN-4 TWN-7 TWN-18 TW4-22* TW4-24* TW4-25* Piezometer 1 Piezometer 2 Piezometer 3 As discussed in Section 2.1.2 the analytical constituents required by the CAP are inorganic chloride and nitrate+nitrite as N (referred to as nitrate in this document) * Wells TW4-22, TW4-24, TW4-25 are chloroform investigation wells (wells installed and sampled primarily for the chloroform investigation) and are sampled as part of the chloroform program. The analytical suite for these three wells includes nitrate, chloride and a select list of Volatile Organic Compounds ("VOCs") as specified in the chloroform program. These three wells are included here because they are being pumped as part of the remediation of the nitrate contamination as required by the SCO and the CAP. The nitrate and chloride data are included in this repmt as well as in the chloroform program quarterly report. The VOC data for these three wells will be reported in the chloroform quarterly monitoring report only. The December 12, 2012 SCO approved the CAP, which specified the cessation of sampling in TWN-5, TWN-6, TWN-8, TWN-9, TWN-10, TWN-11, TWN-12, TWN-13, TWN-14, TWN-15, TWN-16, TWN-17, and TWN-19. The CAP and SCO also approved the abandonment ofTWN- 5, TWN-8, TWN-9, TWN-10, TWN-11, TWN-12, TWN-13, TWN-15, and TWN-17 within 1 year of the SCO approval. These wells were abandoned in accordance with the DRC-approved Well Abandonment Procedure on July 31, 2013. Wells TWN-6, TWN-14, TWN-16, and TWN- 19 have been maintained for depth to groundwater monitoring only, as noted in the CAP. Table 1 provides an overview of all locations sampled during the current period, along with the date samples were collected from each location, and the date(s) upon which analytical data were received from the contract laboratory. Table 1 also identifies rinsate samples collected, as well as sample numbers associated with any required duplicates. As indicated in Table 1, nitrate monitoring was performed in the nitrate monitoring wells, chloroform wells TW4-22, TW4-24, TW4-25 and Piezometers 1, 2, and 3. Analytical data for all of the above-listed wells, and the piezometers, are included in Tab G. Nitrate and chloride are also monitored in all of the Mill's groundwater monitoring wells and chloroform investigation wells. Data from those wells for this quarter are incorporated in certain maps and figures in this report but are discussed in their respective programmatic reports. 2 2.1.2 Parameters Analyzed Locations sampled during this reporting period were analyzed for the following constituents: • Inorganic Chloride • Nitrate plus Nitrite as Nitrogen (referred to herein as nitrate) Use of analytical methods consistent with the requirements found in the White Mesa Mill Groundwater Quality Assurance Plan, ("QAP") Revision 7.2, dated June 6, 2012 was confirmed for all analytes, as discussed later in this report. 2.1.3 Groundwater Head and Level Monitoring Depth to groundwater was measured in the following wells and/or piezometers, pursuant to Part I.E.3 of the Groundwater Discharge Permit ("GWDP") (dated August 24, 2012): • The quarterly groundwater compliance monitoring wells • Existing well MW -4 and all of the temporary chloroform investigation wells • Piezometers-P-1, P-2, P-3, P-4 and P-5 • MW-20, MW-22, and MW-34 • The DR piezometers that were installed during the Southwest Hydrogeologic Investigation • Nitrate wells TWN-1, TWN-2, TWN-3, TWN-4, TWN-6, TWN-7, TWN-14, TWN-16, TWN-18 and TWN-19 In addition to the above, depth to water measurements are routinely observed in conjunction with sampling events for all wells sampled during quarterly and accelerated efforts, regardless of the sampling purpose. All well levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab C. Field data sheets for groundwater measurements are also provided in Tab C. Weekly and monthly depth to groundwater measurements were taken in the chloroform pumping wells MW-4, MW-26, TW4-19, TW4-20, TW4-4, TW4-01, TW4-02, and TW4-11, and the nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2. The UDEQ Groundwater Corrective Action Plan for Chloroform Plume Remediation (the "GCAP") dated December 18, 2014 and awaiting final approval, requires that chloroform monitoring wells TW4-01, TW4-02, and TW4-11 be converted to pumping wells. In anticipation of final approval of the GCAP, EFRI converted TW 4-01, TW 4-02, and TW 4-11 to pumping wells and began pumping on January 14, 2015. In addition, monthly water level measurements were taken in non-pumping wells MW-27, MW- 30, MW-31, TW4-21, TWN-1, TWN-3, TWN-4, TWN-7, and TWN-18 as required by the CAP. 3 2.2 Sampling Methodology and Equipment and Decontamination Procedures The QAP provides a detailed presentation of procedures utilized for groundwater sampling activities under the GWDP (August 24, 2012). The sampling methodology, equipment and decontamination procedures that were performed for the nitrate contaminant investigation, as summarized below, are consistent with the QAP. 2.2.1 Well Purging, Sampling and Depth to Groundwater A list of the wells in order of increasing nitrate contamination is generated quarterly. The order for purging is thus established. The list is included with the Field Data Worksheets under Tab B. Mill personnel start purging with all of the nondetect wells and then move to the wells with detectable nitrate concentrations, progressing from the wells having the lowest nitrate contamination to wells with the highest nitrate contamination. Before leaving the Mill office, the pump and hose are decontaminated using the cleaning agents described in Attachment 2-2 of the QAP. Rinsate blanks are collected at a frequency of one rinsate per 20 field samples. Purging is completed to remove stagnant water from the casing and to assure that representative samples of formation water are collected for analysis. There are three purging strategies specified in the QAP that are used to remove stagnant water from the casing during groundwater sampling at the Mill. The three strategies are as follows: 1. Purging three well casing volumes with a single measurement of field parameters 2. Purging two casing volumes with stable field parameters (within 10% Relative Percent Difference ["RPD"]) 3. Purging a well to dryness and stability (within 10% RPD) of a limited list of field parameters after recovery. Mill personnel proceed to the first well, which is the well with the lowest concentration (i.e. non- dectect) of nitrate based on the previous quarter's sampling results. Well depth measurements are taken and the one casing volume is calculated. The purging strategy that will be used for the well is determined at this time based on the depth to water measurement and the previous production of the well. The Grundfos pump (a 6 to 10 gallon per minute [gpm] pump) is then lowered to the appropriate depth in the well and purging is started. At the first well, the purge rate is measured for the purging event by using a calibrated 5 gallon bucket. After the evacuation of the well has been completed, the well is sampled when possible, and the pump is removed from the well and the process is repeated at each well location moving from the least contaminated to most contaminated well. If sample collection is not possible due to the well being purged dry, a sample is collected after recovery using a disposable bailer and as described in Attachment 2-3 of the QAP. Sample collection follows the procedures described in Attachment 2-4 of the QAP. 4 After the samples have been collected for a patticular well, the samples are placed into a cooler that contains ice. The well is then recapped and Mill personnel proceed to the next well. If a bailer has been used it is disposed of. Decontamination of non-dedicated equipment, using the reagents in Attachment 2-2 of the QAP, is performed between each sample location, and at the beginning of each sampling day, in addition to the pre-event decontamination described above. 2.2.2 Piezometer Sampling Samples are collected from Piezometers 1, 2 and 3, if possible. Samples are collected from piezometers using a disposable bailer after one set of field measurements have been collected. Due to the difficulty in obtaining samples from the piezometers, the purging protocols set out in the QAP are not followed. After samples are collected, the bailer is disposed of and samples are placed into a cooler containing ice for sample preservation and transit to the Mill's contract analytical laboratory, American West Analytical Laboratories ("AWAL"). 2.3 Field Data Attached under Tab B are copies of all Field Data Worksheets that were completed during the quarter for the nitrate investigation monitoring wells and piezometers identified in Section 2.1.1 and Table 1. 2.4 Depth to Groundwater Data and Water Table Contour Map Depth-to-groundwater measurements that were utilized for groundwater contours are included on the Quarterly Depth to Water Sheet at Tab C of this Report along with the kriged groundwater contour map for the current quarter generated from this data. All well levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab C. A copy of the kriged groundwater contour map generated from the previous quarter's data is provided under Tab D. 2.5 Laboratory Results 2.5.1 Copy of Laboratory Results The analytical results were provided by AW AL. Table 1 lists the dates when analytical results were reported to the Quality Assurance ("QA") Manager for each well or other sample. Analytical results for the samples collected for this quarter's nitrate investigation and a limited list of chloroform investigation nitrate and chloride results are provided under Tab G of this Report. AI. o includ~d under Tab G are the results of analyses for duplicate samples and rinsate arnples for thls sampling effo1t, identified in Table 1. See the Groundwater Monitoring Report and Chloroform Monit01ing Report for this quarter for nitrate and chloroform analytical re. ult for the groundwater monitori_og well and chloroform investigation wells not listed in Table 1. 5 2.5.2 Regulatory Framework As discussed in Section 1.0 above, the Request, Plan, and CA each triggered a series of actions on EFRI' s part. Potential surficial sources of nitrate and chloride have been described in the December 30, 2009 CIR and additional investigations into potential sources were completed and discussed with DRC in 2011. Pursuant to theCA, the CAP was submitted to the Director of the Division of Radiation Control (the "Director") on May 7, 2012. The CAP describes activities associated with the nitrate in groundwater. The CAP was approved by the Director on December 12, 2012. This quarterly report documents the monitoring consistent with the program described in the CAP. 3.0 QUALITY ASSURANCEANDDATA VALIDATION EFRI's QA Manager performed a QA/Quality Control ("QC") review to confirm compliance of the monitoring program with the requirements of the QAP. As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and QC review of laboratory data methods and data. Identification of field QC samples collected and analyzed is provided in Section 3 .1. Discussion of adherence to Mill sampling Standard Operating Procedures ("SOPs") is provided in Section 3.2. Analytical completeness review results are provided in Section 3.3. The steps and tests applied to check field data QA/QC, holding times, receipt temperature and laboratory data QA/QC are discussed in Sections 3.4.1 through 3.4.7 below. The analytical laboratory has provided summary reports of the analytical QA/QC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference certification and reporting protocol. The Analytical Laboratory QA/QC Summary Reports, including copies of the Mill's Chain of Custody and Analytical Request Record forms for each set of Analytical Results, follow the analytical results under Tab G. Results of the review of the laboratory QA/QC information are provided under Tab H and discussed in Section 3.4, below. 3.1 Field QC Samples The following QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program. Field QC samples for the nitrate investigation program consist of one field duplicate sample for each 20 samples, DI Field Blanks ("DIFB"), and equipment rinsate samples. During the quarter, one duplicate sample was collected as indicated in Table 1. The duplicate was sent blind to the analytical laboratory and analyzed for the same parameters as the nitrate wells. One rinsate blank sample was collected as indicated on Table 1. Rinsate samples are labeled with the name of the subsequently purged well with a terminal letter "R" added (e.g. TWN-7R). The field QC sample results are included with the routine analyses under Tab G. 6 3.2 Adherence to Mill Sampling SOPs The QA Manager review of Mill Personnel's adherence to the existing SOPs, confirmed that the QNQC requirements established in the QAP and Chloroform QAP were met. 3.3 Analyte Completeness Review All analyses required by the GWDP for nitrate monitoring for the period were performed. 3.4 Data Validation The QAP and GWDP (August 24, 2012) identify the data validation steps and data QC checks required for the nitrate monitoring program. Consistent with these requirements, the QA Manager performed the following evaluations: a field data QNQC evaluation, a holding time evaluation, an analytical method check, a reporting limit evaluation, a QC evaluation of sample duplicates, a QC evaluation of control limits for analysis and blanks, a receipt temperature evaluation, and a rinsate evaluation. Because no VOCs are analyzed for the nitrate contamination investigation, no trip blanks are required in the sampling program. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab H. 3.4.1 Field Data QA/QC Evaluation The QA Manager performs a review of all field recorded parameters to assess their adherence with QAP requirements. The assessment involved review of two sources of information: the Field Data Sheets and the Quarterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and stability of five parameters: conductance, pH, temperature, redox potential, and turbidity. Review of the Depth to Water data confirms that all depth measurements used for development of groundwater contour maps were conducted within a five-day period of each other. The results of this quarter's review are provided under Tab H. Based upon the review of the field data sheets, field work conformed with the QAP purging and field measurement requirements. A summary of the purging techniques employed and field measurements taken is described below: Purging Two Ca ing Volumes with Stable Field Parameter. Cwilhin 10% RPD) Wells TWN-01, TWN-04, and TWN-18 were sampled after two casing volumes were removed. Field parameters pH, specific conductivity, turbidity, water temperature, and redox potential were measured during purging. All field parameters for this requirement were stable within 10% RPD. Purgin!! a Welllo Dryo·e sand lability of a Limited List of Field Param ter · Wells TWN-03 and TWN-07 were purged to dryness before two casing volumes were evacuated. After well recovery, one set of measurements for the field parameters of pH, specific conductivity, and water temperature only were taken; the samples were collected, and another set of measurements for pH, specific conductivity, and water temperature were taken. Stabilization 7 of pH, conductivity and temperature are required within 10% RPD under the QAP. All field parameters for this requirement were stable within 10% RPD. Continuously Pumped Wells Wells TWN-02, TW4-22, TW4-24, and TW4-25 are continuously pumped wells. These wells are pumped on a set schedule per the remediation plan and are considered sufficiently evacuated to immediately collect a sample. As previously noted, TW4-22, TW4-24, and TW4-25 are chloroform investigation wells and are sampled under the chloroform program. Data for nitrate and chloride are provided here for completeness purposes. During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water to the nearest 0.01 foot. All field parameters for all wells were within the QAP required limits, as indicated below. The review of the field sheets for compliance with QAP requirements resulted in the observations noted below. The QAP requirements in Attachment 2-3 specifically state that field parameters must be stabilized to within 10% over at least 2 consecutive measurements for wells purged to two casing volumes or to dryness. The QAP Attachment 2-3 states that turbidity should be less than 5 NTU prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP Attachment 2-3 does not require that turbidity measurements be less than 5 NTU prior to sampling. As such the noted observations regarding turbidity measurements greater than 5 NTU below are included for information purposes only. • All well measurements met the QAP's 5 NTU turbidity goal and all required turbidity RPD's met the QAP Requirement to stabilize within 10%, as noted in Tab H. EFRI's letter to DRC of March 26, 2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In response to DRC' s subsequent correspondence dated June 1, 2010 and June 24, 2010, EFRI completed a monitoring well redevelopment program. The redevelopment report was submitted to DRC on September 30, 2011. DRC responded to the redevelopment report via letter on November 15, 2012. Per the DRC letter dated November 15, 2012, the field data generated this quarter are compliant with the turbidity requirements of the approved QAP. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided in Tab H. All samples were received and analyzed within the required holding time. 3.4.3 Analytical Method Checklist All analytical methods reported by the laboratory were checked against the required methods enumerated in the QAP. Analytical method checks are provided in Tab H. All methods were consistent with the requirements of the QAP. 8 3.4.4 Reporting Limit Evaluation All analytical method reporting limits ("RLs") reported by the laboratory were checked against the reporting limits enumerated in the QAP. Reporting Limit Checks are provided in Tab H. All analytes were measured and reported to the required reporting limits, with the exception of several samples that had increased reporting limits due to matrix interference or required dilution due to the sample concentration. However, in all of those cases the analytical results were greater than the reporting limit used. 3.4.5 QA/QC Evaluation for Sample Duplicates Section 9.1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results are less than 5 times the required detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05- 01 as cited in the QAP. The RPDs are calculated for duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits. However, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPD is greater than 20%. The duplicate results were within a 20% RPD. Results of the RPD test are provided in Tab H. 3.4.6 Other Laboratory QA/QC Section 9.2 of the QAP requires that the laboratory's QNQC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is conect and complete, (3) appropriate Analytical Laboratory procedures are followed, (4) analytical results are conect and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, EFRI's QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided in Tab H. The lab QNQC results met these specified acceptance limits. The QAP Section 8.1.2 requires that a Matrix Spike/Matrix Spike Duplicate ("MS/MSD") pair be analyzed with each analytical batch. The QAP does not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the MS/MSD pair be prepared on EFRI samples only. Acceptance limits for MS/MSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the QAP requirement to analyze an MS/MSD pair with each analytical batch was met. While the QAP does not require it, the recoveries were reviewed for compliance with the laboratory established acceptance limits. The QAP does not require this level of review, and the results of this review are provided for information only. 9 The information from the Laboratory QA/QC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for the samples were within acceptable laboratory limits for the regulated compounds except as indicated in Tab H. The MS/MSD recoveries that are outside the laboratory established acceptance limits do not affect the quality or usability of the data because recoveries above or below the acceptance limits are indicative of matrix interference. Matrix interferences are applicable to the individual sample results only. The requirement in the QAP to analyze a MS/MSD pair with each analytical batch was met and as such the data are compliant with the QAP. The information from the Laboratory QA/QC Summary Reports indicates that the Laboratory Control Sample recoveries were acceptable, which indicate that the analytical system was operating properly. The QAP Section 8.1.2 requires that each analytical batch shall be accompanied by a reagent blank. All analytical batches routinely contain a blank, which is a laboratory-grade water blank sample made and can·ied through all analytical steps. For the Mill samples, a method blank is prepared for all analytical methods. The information from the Laboratory QA/QC Summary Reports indicates that the method blanks did not contain detections of any target analytes above the Reporting Limit. 3.4.7 Receipt Temperature Evaluation Chain of Custody sheets were reviewed to confirm compliance with the QAP requirement in QAP Table 1 that samples be received at 6°C or lower. Sample temperatures checks are provided in Tab H. All samples were received within the required temperature limit. 3.4.8 Rinsate Check Rinsate checks are provided in Tab H. A comparison of the rinsate blank sample concentration levels to the QAP requirements -that rinsate sample concentrations be one order of magnitude lower than that of the actual well -indicated that all of the rinsate blank analytes met this criterion. All rinsate and DIFB blank samples were non-detect for the quarter. 4.0 INTERPRETATIONOFDATA 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions. 4.1.1 Current Site Groundwater Contour Map As stated above, a listing of groundwater level readings for the current quarter (shown as depth to groundwater in feet) is included under Tab C. The data from this tab has been interpreted (interpolated by kriging) and plotted in a water table contour map, provided under the same tab. The contour map is based on the current quarter's data for all wells. The water level contour map indicates that perched water flow ranges from generally southwesterly beneath the Mill site and tailings cells to generally southerly along the eastern and western margins of White Mesa. Perched water mounding associated with the wildlife ponds 10 locally changes the generally southerly perched water flow patterns. For example, northeast of the Mill site, mounding associated with wildlife ponds results in locally northerly flow near PIEZ-1. The impact of the mounding associated with the northern ponds, to which water has not been delivered since March 2012, is diminishing and is expected to continue to diminish as the mound decays due to reduced recharge. Not only has recharge from the wildlife ponds impacted perched water elevations and flow directions at the site, but the cessation of water delivery to the northern ponds, which are generally upgradient of the nitrate and chloroform plumes at the site, has resulted in changing conditions that are expected to impact constituent concentrations and migration rates within the plumes. Specifically, past recharge from the ponds has helped limit many constituent concentrations within the plumes by dilution while the associated groundwater mounding has increased hydraulic gradients and contributed to plume migration. Since use of the northern wildlife ponds ceased in March 2012, the reduction in recharge and decay of the associated groundwater mound are expected to increase many constituent concentrations within the plumes while reducing hydraulic gradients and acting to reduce rates of plume migration. EFRI and its consultants have raised the issues and potential effects associated with cessation of water delivery to the northern wildlife ponds during discussions with DRC in March 2012 and May 2013. The impacts associated with cessation of water delivery to the northern ponds are expected to propagate downgradient (south and southwest) over time. Wells close to the ponds are generally expected to be impacted sooner than wells farther downgradient of the ponds. Therefore, constituent concentrations are generally expected to increase in downgradient wells close to the ponds before increases are detected in wells farther downgradient of the ponds. Although such increases are anticipated to result from reduced dilution, the magnitude and timing of the increases are difficult to predict due to the complex permeability distribution at the site and factors such as pumping and the rate of decay of the groundwater mound. The potential exists for some wells completed in higher permeability materials to be impacted sooner than some wells completed in lower permeability materials even though the wells completed in lower permeability materials may be closer to the ponds. Localized increases in concentrations of constituents such as nitrate and chloride within and near the nitrate plume may occur even when the nitrate plume is under control based on the Nitrate CAP requirements. Ongoing mechanisms that can be expected to increase the concentrations of nitrate and chloride locally as a result of reduced wildlife pond recharge include but are not limited to: 1) Reduced dilution -the m1xmg of low constituent concentration pond recharge into existing perched groundwater will be reduced over time. 2) Reduced saturated thicknesses -dewatering of higher permeability zones rece1vmg primarily low constituent concentration pond water will result in wells intercepting the zones receiving a smaller proportion of the low constituent concentration water. The combined impact of the above two mechanisms may be especially evident at chloroform pumping wells MW-4, MW-26, TW4-4, TW4-19, and TW4-20; nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2; and non-pumped wells adjacent to the pumped wells. The 11 overall impact is expected to be generally higher constituent concentrations in these wells over the short term until mass reduction resulting from pumping and natural attenuation eventually reduce concentrations. In addition to changes in the flow regime caused by reduced wildlife pond recharge, perched flow directions are locally influenced by operation of the chloroform and nitrate pumping wells. As shown in the detail water level map provided under Tab C, well defined cones of depression are evident in the vicinity of all chloroform pumping wells except TW4-4, which began pumping in the first quarter of 2010. Although operation of chloroform pumping well TW4-4 has depressed the water table in the vicinity of TW4-4, a well-defined cone of depression is not clearly evident. The lack of a well-defined cone of depression near TW4-4 likely results from 1) variable permeability conditions in the vicinity of TW4-4, and 2) persistent relatively low water levels at adjacent well TW4-14. Wells TW4-1, TW4-2, and TW4-11 were added to the chloroform pumping network this quarter, and have lowered water levels east of the nitrate plume in the general vicinity of chloroform pumping well MW -4. Decreases in water levels were especially evident at non-pumping wells TW4-7 and TW4-8. Pumping of nitrate wells TW4-22, TW4-24, TW4-25, and TWN-2 began during the first quarter of 2013. Water level patterns near these wells are expected to be influenced by the presence of and the decay of the groundwater mound associated with the northern wildlife ponds, and by the persistently low water level elevation at TWN-7, which is located up gradient of the nitrate pumping wells. Capture associated with nitrate pumping is expected to increase over time as water levels decline due to pumping and to cessation of water delivery to the northern wildlife ponds. Interaction between nitrate and chloroform pumping is expected to enhance the capture of the nitrate pumping system. The long term interaction between the nitrate and chloroform pumping systems will, however, require more data to be collected as part of routine monitoring. As discussed above, variable permeability conditions are one likely reason for the lack of a well- defined cone of depression near chloroform pumping well TW4-4. Changes in water levels at wells immediately south of TW4-4 resulting from TW4-4 pumping are expected to be muted because TW4-4 is located at a transition from relatively high to relatively low permeability conditions south (downgradient) of TW4-4. The permeability of the perched zone at TW4-6 and TW4-26, and recently installed wells TW4-29, TW4-30, TW4-31, TW4-33, TW4-34, and TW4- 35 is one to two orders of magnitude lower than at TW4-4. Any drawdown of water levels at wells immediately south of TW4-4 resulting from TW4-4 pumping is also difficult to determine because of the general, long-term increase in water levels in this area that resulted from wildlife pond recharge. Water levels at TW4-4 and TW4-6 increased by nearly 2.7 and 2.9 feet, respectively, between the fourth quarter of 2007 and the fourth quarter of 2009 (just prior to the start of TW 4-4 pumping) at rates of approximately 1.2 feet/year and 1.3 feet/year, respectively. However, the rate of increase in water level at TW4-6 after the start of pumping at TW4-4 (first quarter of 2010) was reduced to less than 0.5 feet/year suggesting that TW4-6 is within the hydraulic 12 influence of TW 4-4. Furthermore, water levels at TW 4-6 have been trending downward since the fourth quarter of 20 13 suggesting an additional influence related to the cessation of water delivery to the northern wildlife ponds as discussed above. (note: hydrographs for these wells are provided in the quarterly Cbl rofonn Moni toring Report). Rccharg from the southern wildlife pond is expe ted l continue to have an ffect on ater level near TW 4-4 even as the groundwater mound as ·o iated with recharge from lhe norlhern ponds diminishes over time due to cessation of water delivery to those ponds. The lack of a well-defined cone of depression at TW4-4 is also influenced by the persistent, relatively low water level at non-pumping well TW4-14, located east ofTW4-4 and TW4-6. For the current quarter, the water level at TW4-14 was measured at approximately 5530.9 feet above mean sea level ("ft amsl"). This is approximately 7 feet lower than the water level at TW 4-6 (approximately 5538.0 ft amsl) and 11 feet lower than the water level at TW4-4 (approximately 5541.5 ft amsl) even though TW4-4 is pumping. Well TW4-27 (installed south of TW4-14 in the fourth quarter of 2011) has a static water level of approximately 5527.7 ft amsl, similar to TW4-14 (approximately 5530.9 ft amsl). Prior to the installation of TW4-27, the persistently low water level at TW4-14 was considered anomalous because it appeared to be downgradient of all three wells TW4-4, TW4-6, and TW4-26, yet chloroform had not been detected at TW4-14. Chloroform had apparently migrated from TW4-4 to TW4-6 and from TW4-6 to TW4-26 which suggested that TW4-26 was actually downgradient of TW4-6, and TW4-6 was actually downgradient of TW4-4, regardless of the flow direction implied by the low water level at TW4-14. The water level at TW4-26 (5536.4 feet amsl) is, however, lower than water levels at adjacent wells TW4-6 (5538.0 feet amsl), and TW4-23 (5539.5 feet amsl), as shown in the detail water level map under Tab C. Hydraulic tests indicate that the permeability at TW4-27 is an order of magnitude lower than at TW4-6 and three orders of magnitude lower than at TW4-4 (see Hydro Geo Chern, Inc. [HGC], September 20, 2010: Hydraulic Testing of TW4-4, TW4-6, and TW4-26, White Mesa Uranium Mill, July 2010; and HGC, November 28, 2011: Installation, Hydraulic Testing, and Perched Zone Hydrogeology of Perched Monitoring Well TW4-27, White Mesa Uranium Mill Near Blanding, Utah). The similar water levels at TW4-14 and TW4-27, and the low permeability estimate at TW4-27 suggest that both wells are completed in materials having lower permeability than nearby wells. The low permeability condition likely reduced the rate of long-term water level increase at TW4-14 and TW4-27 compared to nearby wells, yielding water levels that appeared anomalously low. This behavior is consistent with hydrauli t l data c llected from recently installed wells TW4-29, TW4-30, TW4-31, TW4-33 and TW4-34 which indicate that the permeability of these wells is one to two orders of magnitude higher Lhan the permeability of TW4-27 (see HGC, January 23, 2014; Contamination Investigation Report, TW4-12 and TW4- 27 Areas, White Mesa Uranium Mill Near Blanding, Utah; and HGC, July 1, 2014, Installation and Hydraulic Testing of TW4-35 and TW4-36, White Mesa Uranium Mill Near Blanding, Utah [As-Built Report]). Hydraulic tests also indicate that the permeability at TW4-36 is slightly higher than but comparable to the low permeability at TW4-27, suggesting that TW4-36, TW4- 14 and TW4-27 are completed in a continuous low permeability zone. 13 4.1.2 Comparison of Current Groundwater Contour Map to Groundwater Contour Map for Previous Quarter The groundwater contour maps for the Mill site for the previous quarter, as submitted with the Nitrate Monitoring Report for the previous quarter, are attached under Tab D. A comparison of the water table contour maps for the current quarter (first quarter of 2015) to the water table contour maps for the previous quarter (fourth quarter of 2014) indicates relatively large draw downs (decreases in water levels) associated with operation of new chloroform pumping wells TW 4-1, TW 4-2, and TW 4-11. Smaller increases in draw down occun·ed at nearby chloroform pumping wells MW-4 and TW4-4. Drawdowns associated with chloroform pumping wells TW4-19 and TW4-20 decreased this quarter. Nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2 were brought into operation during the first quarter of 2013 and their impact on water level patterns was evident as of the fourth quarter of 2013. While water levels in nitrate pumping well TW4-22 showed a decrease, the water levels at TW4-24, TW4-25, and TWN-2 showed increases this quarter. As discussed in Section 4.1.1, pumping at chloroform well TW 4-4, which began in the first quarter of 2010, has depressed the water table near TW 4-4, but a well-defined cone of depression is not clearly evident, likely due to variable permeability conditions near TW4-4 and the persistently low water level at adjacent well TW4-14. Small ( <1 foot) changes in water levels were reported at the majority of site wells; water levels and water level contours for the site have not changed significantly since the last quarter except for a few locations primarily in the vicinity of the new chloroform pumping wells. Reported decreases in water levels (increases in drawdown) of approximately 4.2, 7.1, 2.2, 31, and 12 feet occurred in chloroform pumping wells TW4-1, TW4-2, TW4-4, and TW4-11, and nitrate pumping well TW4-22, respectively. Increases in water level (decreases in drawdown) of approximately 6.9, 5, 6.3, and 6.3 feet were reported for chloroform pumping wells MW-26, TW4-19, TW4-20, and nitrate pumping well TW4-25, respectively. Changes in water levels at other pumping wells (chloroform pumping well MW-4 and nitrate pumping well TW4-24) were less than 1 foot. Water level fluctuations at pumping wells typically occur in part because of fluctuations in pumping conditions just prior to and at the time the measurements are taken. Although increases in water levels (decreases in drawdown) occurred in some pumping wells and decreases in water levels (increases in drawdown) occurred in others, and new chloroform pumping wells TW4-1, TW4-2, and TW4-11 were brought online, the overall apparent capture of the combined system is about the same as last quarter. Reported water level decreases of less than 1 foot at Piezometers 1 through 3, TWN-1, TWN-4, TWN-6, TWN-18, and MW-19 may result from cessation of water delivery to the northern wildlife ponds as discussed in Section 4.1.1 and the consequent continuing decay of the associated perched water mound. Reported water level decreases of approximately 1.2 feet and 1.4 feet at Piezometers 4 and 5, respectively, may result from reduced recharge at the southern wildlife pond. 14 Reported water levels increased by approximately 4.3 feet at MW-20 and by approximately 2.5 feet at MW-37 between the previous quarter and the current quarter. Water level variability at these wells is likely the result of low permeability and variable intervals between purging/sampling and water level measurement. An increase in water level of approximately 2.9 feet was reported at DR-17; a similar decrease was reported last quarter. Water level decreases of approximately 4 feet and 8 feet at TW4-7 and TW4-8, respectively, are likely the result of the start -up of pumping at TW 4-1, TW 4-2, and TW 4-11. 4.1.3 Hydrographs Attached under Tab E are hydrographs showing groundwater elevation in each nitrate contaminant investigation monitor well over time. Per the CAP, nitrate wells TWN-6, TWN-14, TWN-16, and TWN-19 have been maintained for depth to groundwater monitoring only. These hydrographs are also included in Tab E. 4.1.4 Depth to Groundwater Measured and Groundwater Elevation Attached in Tab F are tables showing depth to groundwater measured and groundwater elevation over time for each of the wells listed in Section 2.1.1 above. 4.2 Effectiveness of Hydraulic Containment and Capture 4.2.1 Hydraulic Containment and Control The CAP states that hydraulic containment and control will be evaluated in part based on water level data and in part on concentrations in wells downgradient of pumping wells TW4-22 and TW4-24. As per the CAP, the fourth quarter of 2013 was the first quarter that hydraulic capture associated with nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2 was evaluated. Hydraulic containment and control based on water level data is considered successful per the CAP if the entire nitrate plume upgradient of TW4-22 and TW4-24 falls within the combined capture of the nitrate pumping wells. Capture zones based on water level contours calculated by kriging the current quarter's water level data are provided on water level contour maps included under Tab C. The nitrate capture zones are defined by the bounding stream tubes associated with nitrate pumping wells. Each bounding stream tube represents a flow line parallel to the hydraulic gradient and therefore perpendicular to the intersected water level contours. Assuming that the stream tubes do not change over time, all flow between the bounding stream tubes associated with a particular pumping well is presumed to eventually reach and be removed by that well. Capture associated with chloroform pumping wells is also included on these maps because the influence of the chloroform and nitrate pumping systems overlap. The specific methodology for calculating the nitrate capture zones is substantially the same as that used since the fourth quarter of 2005 to calculate the capture zones for the chloroform program, as agreed to by the DRC and International Uranium (USA) Corp. The procedure for calculating nitrate capture zones is as follows: 15 1) Calculate water level contours by gridding the water level data on approximately 50-foot centers using the ordinary linear kriging method in Surfer™. Default kriging parameters are used that include a linear variogram, an isotropic data search, and all the available water level data for the quarter, including relevant seep and spring elevations. 2) Calculate the capture zones by hand from the kriged water level contours following the rules for flow nets: -from each pumping well, reverse track the stream tubes that bound the capture zone of each well, -maintain perpendicularity between each stream tube and the kriged water level contours. Compared to last quarter, both increases and decreases in water levels occurred at nitrate and chloroform pumping wells. The water level in nitrate pumping well TW4-22 decreased by nearly 12 feet. Water levels in nitrate pumping wells TW4-24, TW4-25, and TWN-2 increased by approximately 1 foot, 6 feet, and 4 feet, respectively. The water levels in chloroform pumping wells MW-4, TW4-1, TW4-2, TW4-4, and TW4-11 decreased by approximately 1 foot, 4 feet, 7 feet, 2 feet, and 31 feet, respectively, while water levels in chloroform pumping wells MW -26, TW4-19, and TW4-20 increased by approximately 7 feet, 5 feet, and 6 feet, respectively. While the apparent capture of the combined pumping systems has expanded in some areas and been reduced in others, the overall capture is about the same as last quarter. The capture associated with nitrate pumping wells is expected to increase over time as water levels continue to decline due to pumping and to cessation of water delivery to the northern wildlife ponds. Slow development of hydraulic capture is consistent with and expected based on the relatively low permeability of the perched zone at the site. Furthermore, the presence of the perched groundwater mound, and the apparently anomalously low water level at TWN-7, will influence the definition of capture associated with the nitrate pumping system. That pumping is likely sufficient to eventually capture the entire plume upgradient of TW4-22 and TW4-24 can be demonstrated by comparing the combined average pumping rates of all nitrate pumping wells for the current quarter to estimates of pre-pumping flow through the nitrate plume near the locations of TW4-22 and TW4-24. The pre-pumping flow calculation is assumed to represent a steady state 'background' condition that includes constant recharge, hydraulic gradients, and saturated thicknesses, and does not account for reduced recharge and saturated thickness caused by cessation of water delivery to the northern wildlife ponds since March, 2012. Changes after pumping are conservatively assumed to result only from pumping. As will be discussed below, the average combined nitrate pumping rate for the quarter is within the calculated pre-pumping range of perched water flow through the nitrate plume. The cumulative volume of water removed by TW4-22, TW4-24, TW4-25, and TWN-2 during the current quarter was approximately 233,211 gallons. This equates to an average total extraction rate of approximately 1.8 gpm over the 90 day quarter. This average accounts for time periods when pumps were off due to insufficient water columns in the wells and accounts for the extended pumping outage discussed in Section 5. In part due to this outage, the volume of water removed by nitrate pumping was approximately 33% lower than last quarter. In addition to periodic outages resulting from unavoidable equipment downtime, achievable pumping rates are 16 likely to diminish over time as saturated thicknesses are reduced by pumping and by cessation of water delivery to the northern wildlife ponds. Pre-pumping flow through the nitrate plume near TW4-22 and TW4-24 was estimated using Darcy's Law to lie within a range of approximately 1.31 gpm to 2.79 gpm. Calculations were based on an average hydraulic conductivity range of 0.15 feet per day (ft/day) to 0.32 ft/day (depending on the calculation method), a pre-pumping hydraulic gradient of 0.025 feet per foot (ftlft), a plume width of 1,200 feet, and a saturated thickness (at TW4-22 and TW4-24) of 56 feet. The hydraulic conductivity range was estimated by averaging the results obtained from slug test data that were collected automatically by data loggers from wells within the plume and analyzed using the KGS unconfined slug test solution available in Aqtesolve™ (see Hydro Geo Chern, Inc. [HGC], August 3, 2005: Perched Monitoring Well Installation and Testing at the White Mesa Uranium Mill, April Through June 2005; HGC, March 10, 2009: Perched Nitrate Monitoring Well Installation and Hydraulic Testing, White Mesa Uranium Mill; and HGC, March 17 2009: Letter Report to David Frydenlund, Esq, regarding installation and testing of TW4-23, TW4-24, and TW4-25). These results are summarized in Table 6. Data from fourth quarter 2012 were used to estimate the pre-pumping hydraulic gradient and saturated thickness. These data are also summarized in Tables 7 and 8. The average hydraulic conductivity was estimated to lie within a range of 0.15 ftlday to 0.32 ft/day. Averages were calculated four ways. As shown in Table 6 arithmetic and geometric averages for wells MW-30, MW-31, TW4-22, TW4-24, TW4-25, TWN-2, and TWN-3 were calculated as 0.22 and 0.15 ft/day, respectively. Arithmetic and geometric averages for a subset of these wells (MW-30, MW-31, TW4-22, and TW4-24) were calculated as 0.32 and 0.31 ftlday, respectively. The lowest value, 0.15 ft/day, represented the geometric average of the hydraulic conductivity estimates for all the plume wells. The highest value, 0.32 ft/day, represented the arithmetic average for the four plume wells having the highest hydraulic conductivity estimates (MW-30, MW-31, TW4-22, and TW4-24). Pre-pumping hydraulic gradients were estimated at two locations; between TW4-25 and MW-31 (estimated as 0.023 ft/ft), and between TWN-2 and MW-30 (estimated as 0.027 ft/ft). These results were averaged to yield the value used in the calculation (0.025 ft/ft). The pre-pumping saturated thickness of 56 feet was an average of pre-pumping saturated thicknesses at TW4-22 and TW4-24. The hydraulic gradient and saturated thickness used in the calculations are assumed to represent a steady state 'background' condition. However, assumption of a steady state 'background' is inconsistent with the cessation of water delivery to the northern wildlife ponds, located upgradient of the nitrate plume. Hydraulic gradients and saturated thicknesses within the plume are declining as a result of two factors: reduced recharge from the ponds, and the effects of nitrate pumping. Separating the impacts of nitrate pumping from the impacts of reduced recharge from the ponds is problematic. Should pumping cease and 'background' conditions be allowed to re-establish, however, smaller hydraulic gradients and saturated thicknesses would be expected due to reduced recharge, which would lower estimates of 'background' flow. As a result, the 'background' flow calculated using the hydraulic gradient of 0.025 ft/ft and saturated thickness of 56 feet is considered conservatively large. Furthermore, using the 17 arithmetic average hydraulic conductivity of a subset of plume wells having the highest conductivities is considered less representative of actual conditions than using the geometric average conductivity of all of the plume wells. Therefore nitrate pumping likely exceeds flow through the plume by a factor greater than 1.4, the high end of the calculated range. The CAP states that MW-5, MW-11, MW-30, and MW-31 are located downgradient ofTW4-22 and TW4-24. MW-30 and MW-31 are within the plume near its downgradient edge and MW-5 and MW-11 are outside and downgradient of the plume. Per the CAP, hydraulic control based on concentration data will be considered successful if the concentrations of nitrate in MW -30 and MW -31 remain stable or decline, and concentrations of nitrate in downgradient wells MW -5 and MW -11 do not exceed the 10 mg/L standard. Table 5 presents the nitrate concentration data for MW-30, MW-31, MW-5 and MW-11, which are down-gradient of pumping wells TW4-22 and TW4-24. Based on these concentration data, the nitrate plume is under control. The plume has not migrated downgradient to MW -5 or MW -11 because nitrate was not detected at MW-11 and was detected at a concentration of only 0.2 mg/L at MW-5 last quarter. Between the previous and current quarters, nitrate concentrations decreased in both MW -30 and MW -31. Nitrate in MW-30 decreased from 16.2 mg/L to 14.9 mg/L and nitrate in MW-31 decreased from 20.9 mg/L to 18.7 mg/L. Although short-term fluctuations have occurred, nitrate concentrations in MW-30 and MW-31 have been relatively stable, demonstrating that plume migration is minimal or absent. Chloride has been relatively stable at MW-30 but is generally increasing at MW-31 (see Tab J and Tab K, discussed in Section 4.2.4). The apparent increase in chloride and stable nitrate at MW -31 suggests a natural attenuation process that is affecting nitrate but not chloride. A likely process that would degrade nitrate but leave chloride unaffected is reduction of nitrate by pyrite. The likelihood of this process in the perched zone is discussed in HGC, December 7 2012; Investigation of Pyrite in the Perched Zone, White Mesa Uranium Mill Site, Blanding, Utah. 4.2.2 Current Nitrate and Chloride Isoconcentration Maps Included under Tab I of this Report are current nitrate and chloride iso-concentration maps for the Mill site. Nitrate iso-contours start at 5 mg/L and chloride iso-contours start at 100 mg/L because those values appear to separate the plumes from background. All nitrate and chloride data used to develop these iso-concentration maps are from the current quarter's sampling events. 4.2.3 Comparison of Areal Extent The increase in nitrate concentrations in TW4-25 from approximately 1 mg.L to 14 mg/L has expanded the plume to the northeast and brought TW4-25 back within the plume. TW4-25 was outside the plume from the first quarter of 2013 through last quarter (see Tab J and Tab K, discussed in Section 4.2.4). The increase in concentration at TW4-24 is likely the result of reduced wildlife pond dilution. 18 The nitrate concentration at TW4-18 (located east of the nitrate plume) increased slightly from 11.1 mg/L to 11.7 mg/L. Changes in nitrate concentrati n near TW4-I are expe , ted to resull from changes in pumping and from the ce sati "'of water delivery to the n rlhern wj.ldlife p ncl . The reduction in low-nitrate recharge from the p . nds appeared to be ha ing th ·anticipated effect of generally increru eel nitrate concemrati n in wells downgrad ienL of the pond . However decreasing to li lati ve ly ·tabJe nitrate concentrations at most wells in the vicinity ofTW4-18 over the previous f, ur quarter after pre i u · increases suggests that conditions in this area have stabilized. All bot gh increase · in concemratjon in the area downgradient of the wildlife ponds have been ant icipated a the re . .ult of reduced di luti n, the magnitude and timing of the increases are dif ficult to p1·edict due to the measured variation in hydraulic conductivity at the site and other factors. Nitrate in th e area di rectly d \Vn,gradient (south to south-southwest) of the northern wildlife ponds is associated with the chloroform plume, is cross-gradient of the nitrate plume as defined in the CAP, and is within the capture zone of the chloroform pumping system (primarily chloroform pumping well MW-26). Perched water flow in the area is to the southwest in the same approximate direction as the main body of the nitrate plume. Nitrate concentrations at the downgradient edge f lhe plume (MW-30 and MW-31) continue to be relatively stable, demonstrating that plume migration i minimaJ or b ent. With regard t chloroform, since the initiation of nitrate pumpin0 the boundary f the chlor form plum bas migrated to the west toward nitrate pumping well TW4-24 and more recently ha migrated ro the southwest to reincorporate chloroform monitoring wells TW4-6 and TW4-16. More details regarding the chloroform data and interpretation are included in the Quarterly Chloroform Monitoring Report submitted under separate cover. 4.2.4 Nitrate and Chloride Concentration Trend Data and Graphs Attached under Tab J is a table summarizing values for nitrate and chloride for each well over time. Attached under Tab K are graphs showing nitrate and chloride concentration plots in each monitor well over time. 4.2.5 Interpretation of Analytical Data Comparing the nitrate analytical results to those of the previous quarter, as summarized in the tables included under Tab J, the following observations can be made for wells within and immediately surrounding the nitrate plume: a) Nitrate concentrations have increased by more than 20% in the following wells compared to last quarter: MW-26, TW4-19, TW4-20, TW4-22, and TW4-25; b) Nitrate concentrations have decreased by more than 20% in the following wells compared to last quarter: MW-27, TW4-16, TWN-2 and TWN-18; c) Nitrate concentrations have remained within 20% in the following wells compared to last quarter: MW-30, MW-31, TW4-21, TW4-24, TWN-1, TWN-3, TWN-4 and TWN- 7;and 19 d) MW-11, MW-25, and MW-32 remained non-detect As indicated, nitrate concentrations for many of the wells with detected nitrate were within 20% of the values reported during the previous quarter, suggesting that variations are within the range typical for sampling and analytical error. The remaining wells had changes in concentration greater than 20%. The latter includes chloroform pumping wells MW-26, TW4-19, and TW4-20; nitrate pumping wells TW4-22, TW4-25 and TWN-2; and non-pumping wells MW-27, TW4-16, and TWN-18. MW-27 is located adjacent to nitrate pumping well TWN-2; and TW4-16 is located adjacent to chloroform pumping well MW-26. Fluctuations in concentrations at pumping wells and wells adjacent to pumping wells likely result in part from the effects of pumping as discussed in Section 4.1.1. Concentrations at TWN-18 are expected to be influenced by its location immediately up gradient of the nitrate plume. As discussed in Section 4.2.3, the nitrate concentration at TW4-25 increased from approximately 1 mg/L last quarter to approximately 14 mg/L this quarter, bringing it again within the nitrate plume boundary. The nitrate concentrations in chloroform pumping wells MW-26, TW4-19, and TW4-20 increased from approximately 1.1 mg/L, 4.7 mg/L and 7.7 mg/L, respectively, to approximately 2.7 mg/L, 8.6 mg/L, and 9.8 mg/L, respectively. MW-27, located west of TWN- 2, and TWN-18, located north of TWN-3, bound the nitrate plume to the west and north (See Figure 1-1 under Tab 1). In addition, the southernmost (downgradient) boundary of the plume remains between MW-30/MW-31 and MW-5/MW-11. Nitrate concentrations at MW-5 (adjacent to MW-11) and MW-11 have historically been low (< 1 mg/L) or non-detect for nitrate (See Table 5). MW-25, MW-26, MW-32, TW4-16, TW4-19, TW4-20, TWN-1, and TWN-4 bound the nitrate plume to the east. As discussed above, the areal extent of the plume has expanded to the northeast to re-encompass TW4-25. Nitrate concentrations outside the nitrate plume exceed 10 mg/L at a few locations: TW4-10 (15 mg/L), TW4-12 (19.2 mg/L), TW4-18 (11.7 mg/L), TW4-26 (14.4 mg/L), TW4-27 (26.5 mg/L), and TW4-28 (19 mg!L). All these wells are located southeast of the nitrate plume as defined in the CAP and all are separated from the plume by wells having nitrate concentrations that are either non-detect, or, if detected, are less than 10 mg/L. Concentrations at TW4-10, TW4-12, TW4-18, TW4-26, TW4-27 and TW4-28 are within 20% of their concentrations during the previous quarter.. From the third quarter of 2013 through the second quarter of 2014, nitrate concentrations at TW 4-10 and TW 4-18 exceeded 10 mg/L, dropped below 10 mg/L in the third quarter of 2014, then increased above 10 mg/L last quarter. Elevated nitrate concentrations at these wells are associated with the chloroform plume, and both are within the capture zone of the chloroform pumping system. Elevated nitrate at TW4-12, TW4-26, TW4-27, and TW4-28 is likely related to former cattle ranching operations at the site. Chloride concentrations are measured because elevated chloride (greater than 100 mg/L) is associated with the nitrate plume. Chloride concentrations at all sampled locations this qumter are within 20% of their respective concentrations during the previous quarter except at MW-26, TW4-16, TW4-19, and TW4-25. These changes likely result from changes in pumping. 20 4.3 Estimation of Pumped Nitrate Mass and Residual Nitrate Mass within the Plume Nitrate mass removed by pumping is summarized in Table 2, and includes mass removed by both chloroform and nitrate pumping wells. Table 3 shows the volume of water pumped at each well and Table 4 provides the details of the nitrate removal for each well. Mass removal calculations begin with the third quarter of 2010 because the second quarter, 2010 data were specified to be used to establish a baseline mass for the nitrate plume. As stated in the CAP, the baseline mass is to be calculated using the second quarter, 2010 concentration and saturated thickness data "within the area of the kriged 10 mg/L plume boundary." The second quarter, 2010 data set was considered appropriate because "the second quarter, 2010 concentration peak at TWN-2 likely identifies a high concentration zone that still exists but has migrated away from the immediate vicinity of TWN-2." As shown in Table 2, a total of approximately 1,256 lb of nitrate has been removed from the perched zone since the third quarter of 2010. Prior to the first quarter of 2013, all direct nitrate mass removal resulted from operation of chloroform pumping wells MW-4, MW-26, TW4-4, TW4-19, and TW4-20. During the current quarter: • A total of approximately 82.6 lb of nitrate was removed by the chloroform pumping wells and by nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2. • Of the 82.6 lb removed during the current quarter, approximately 67 lb, (or 81 % ), was removed by the nitrate pumping wells. Baseline mass and current quarter mass estimates (nitrate + nitrite as N) for the nitrate plume are approximately 43,700 lb and 38,742 lbs, respectively. Mass estimates were calculated within the plume boundaries as defined by the kriged 10 mg/L isocon by 1) gridding (kriging) the nitrate concentration data on 50-foot centers; 2) calculating the volume of water in each grid cell based on the saturated thickness and assuming a porosity of 0.18; 3) calculating the mass of nitrate+nitrite as N in each cell based on the concentration and volume of water for each cell; and 4) totaling the mass of all grid cells within the 10 mg/L plume boundary. Data used in these calculations included data from wells listed in Table 3 of the CAP. The nitrate mass estimate for the current quarter is lower than the baseline estimate by 4,958 lb, and this difference is greater than the amount of nitrate mass removed directly by pumping. Changes in the quarterly mass estimates are expected to result primarily from 1) nitrate mass removed directly by pumping, 2) natural attenuation of nitrate, and 3) changes in nitrate concentrations in wells within the plume as a result of re-distribution of nitrate within the plume and changes in saturated thicknesses. Redistribution of nitrate within the plume and changes in saturated thicknesses will be impacted by changes in pumping and in background conditions such as the decay of the perched water mound associated with the northern wildlife ponds. Cessation of water delivery to the northern wildlife ponds is expected to result in reduced saturated thicknesses and reduced dilution, which in turn is expected to result in increases in concentrations. The mass estimate during the current quarter (38,742 lb) was larger than the mass estimate during the previous quarter (34,370 lb) by 4,372 lb or 12.7 %. This difference results primarily 21 from the increase in concentration at TW4-25, which increased the areal extent of the plume compared to last quarter. Nitrate mass removal by pumping and natural attenuation (expected to result primarily from pyrite oxidation/nitrate reduction) act to lower nitrate mass within the plume. Changes resulting from redistribution of nitrate within the plume are expected to result in both increases and decreases in concentrations at wells within the plume and therefore increases and decreases in mass estimates based on those concentrations, thus generating 'noise' in the mass estimates. Furthermore, because the sum of sampling and analytical error is typically about 20%, changes in the mass estimates from quarter to quarter of up to 20% could result from typical sampling and analytical enor alone. Only longer-term analyses of the mass estimates that minimize the impacts of these quarter to quarter variations will provide useful information on plume mass trends. Over the long term, nitrate mass estimates are expected to trend downward as a result of direct removal by pumping and through natural attenuation. As specified in the CAP, once eight quarters of data are collected (starting with the first quarter of 2013), a regression trend line is to be applied to the quarterly mass estimates and evaluated. The trend line is then to be updated quarterly and reevaluated as additional quarters of data are collected. The evaluation will determine whether the mass estimates are increasing, decreasing, or stable. As the previous quarter constituted the eighth quarter as specified in the CAP, the mass estimates were plotted, and a regression line was fitted to the data and evaluated .. The regression line was updated this quarter as shown in Figure M.1 of Tab M. The fitted line shows a decreasing trend in the mass estimates. 5.0 LONG TERM PUMP TEST AT TWN-02, TW4-22, TW4-24, and TW4- 25 OPERATIONS REPORT 5.1 Introduction Beginning in January 2013, EFRI began long term pumping of TW4-22, TW4-24, TW4-25, and TWN-02 as required by the Nitrate CAP, dated May 7, 2012 and the SCO dated December 12, 2012. In addition, as a part of the investigation of chloroform contamination at the Mill site, EFRI has been conducting a Long Term Pump Test on MW-4, TW4-19, MW-26, and TW4-20, and, since January 31, 2010, TW4-4. As mentioned in Section 2.1.3 above, on January 14, 2015, wells TW4-01, TW4-02, and TW4-11 began pumping pursuant to the requirements in the GCAP which is awaiting final approval. The purpose of the test is to serve as an interim action that will remove a significant amount of chloroform-contaminated water while gathering additional data on hydraulic properties in the area of investigation. Because wells MW-4, TW4-19, MW-26, TW4-4, TW4-20, TW4-01, TW4-02, and TW4-11 are pumping wells that may impact the removal of nitrate, they are included in this report and any nitrate removal realized as prut of this pumping is calculated and included in the quarterly reports. 22 The following information documents the operational activities during the quarter. 5.2 Pumping Well Data Collection Data collected during the quarter included the following: • Measurement of water levels at MW-4, TW4-19, MW-26, and TW4-20 and, commencing regularly on March 1, 2010, TW4-4, on a weekly basis, • Measurement of water levels weekly at TW4-22, TW4-24, TW4-25, and TWN-02 commencing January 28, 2013, • Measurement of water levels weekly at TW4-01, TW4-02, and TW4-11 commencing on January 14, 2015, and on a monthly basis selected temporary wells and permanent monitoring wells. • Measurement of pumping history, including: pumping rates total pumped volume operational and non-operational periods. • Periodic sampling of pumped water for chloroform and nitrate/nitrite analysis and other constituents 5.3 Water Level Measurements Beginning August 16, 2003, water level measurements from chloroform pumping wells MW-4, MW-26, and TW4-19 were conducted weekly. From commencement of pumping TW4-20, and regularly after March 1, 2010 for TW4-4, water levels in these two chloroform pumping wells have been measured weekly. From commencement of pumping in January 2013, water levels in wells TW4-22, TW4-24, TW4-25, and TWN-02 have been measured weekly. Copies of the weekly Depth to Water monitoring sheets for MW-4, MW-26, TW4-19, TW4-20, TW4-4, TW4- 22, TW4-24, TW4-25, TWN-02, TW4-01, TW4-02, and TW4-11 are included under Tab C. Monthly depth to water monitoring is required for all of the chloroform contaminant investigation wells and non-pumping wells MW-27, MW-30, MW-31, TW4-21, TWN-1, TWN- 3, TWN-4, TWN-7, and TWN-18. Copies of the monthly depth to Water monitoring sheets are included under Tab C. 5.4 Pumping Rates and Volumes The pumping wells do not pump continuously, but are on a delay device. The wells purge for a set amount of time and then shut off to allow the well to recharge. Water from the pumping wells is either transferred to the Cell 1 evaporation pond or is used in the Mill process. The pumped wells are fitted with a flow meter which records the volume of water pumped from the well in gallons. The flow meter readings shown in Tab C are used to calculate the gallons of water pumped from the wells each quarter as required by Section 7 .2.2 of the CAP. The average pumping rates and quarterly volumes for each of the pumping wells are shown in Table 3. The cumulative volume of water pumped from each of the wells is shown in Table 4. 23 Specific operational problems observed with the well or pumping equipment which occurred during the quarter are noted for each well below in Sections 5.4.1 through 5.4.4. The following issue was noted as affecting multiple wells in the pumping network and is not repeated under the Section for each well. On December 29, 2014, an unscheduled down time occurred which lasted more than 24 hours. The down time was the caused by frozen transfer lines resulting from system/discharge line upgrades. The upgrades were necessary to add three more continuous pumping wells to the chloroform pumping network. The up-sizing of the discharge line required that the old l-inch lines be excavated while the 4-inch lines were connected. During the excavation the l-inch lines, which were still connected to the existing pumping system, were exposed to the elements in the open trench. The Mill experienced below freezing temperatures for most of the week prior to December 29, 2014. The down time during construction caused six continuous pumping wells (MW-04, MW-26, TW4-04, TW4-20, TW4-22, and TW4-24) to be off (not pumping) until the completion of construction. Initial notice of this outage was given by telephone to DRC at approximately 1:00 pm on Monday December 29, 2014 (within 24 hours of discovery). As required by the O&M Plan, a 5-day written notification was also provided to DRC on January 5, 2015. The pumps were returned to service on January 9, 2015. Unless specifically noted below, no additional operational problems were observed with the well or pumping equipment during the quarter. 5.4.1 TW4-19 On January 12, 2015, Mill Field Personnel noted that the pump stopped working in TW4-19. The outage was a result of the discharge line upgrade/upsizing necessary to add TW4-0l, TW4-02, and TW 4-11 to the chloroform pumping network. The discharge line for TW 4-19 was inadvertently damaged during the upsizing activities. Details regarding the upsizing activities are provided in the notification provided to DRC on January 5, 2015. The damage to the discharge line for TW4-19 caused back pressure, which caused the pump in TW4-19 to stop. The outage due to the damage lasted approximately 48 hours. Rather than repair the line, TW4- 19 was connected to the upsized discharge line used for six other wells in the vicinity. As required by the O&M Plan, DRC was notified via telephone on Tuesday, January 13, 2015 within 24 hours of discovery. EFRI provided further documentation of the outage via e-mail on January 15, 2015 when the system had returned to full functionality. 5.4.2 TW 4-02 On February 16, 2015, Mill Field Personnel noted experienced a power outage at TW4-02 during the routine weekly inspection. The Mill Electricians were notified and the power was restored to the well the same day. No official notifications to DRC were required as the issue was rectified within 24-hours. 24 6.0 CORRECTIVE ACTION REPORT There are no corrective actions required during the current monitoring period. 6.1 Assessment of Previous Quarter's Corrective Actions There were no corrective actions required during the previous quarters' monitoring period. 7.0 CONCLUSIONS AND RECOMMENDATIONS As per the CAP, the current quarter is the sixth quarter that hydraulic capture associated with nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2 was evaluated. Although chloroform wells TW4-1, TW4-2, and TW4-11 began pumping this quarter and increased capture in the vicinity of MW -4, water level monitoring indicates that the apparent combined capture area of the nitrate and chloroform pumping systems is similar to last quarter. Capture associated with nitrate pumping wells continues to develop and is expected to increase over time as water levels decline due to pumping and to cessation of water delivery to the northern wildlife ponds. Furthermore, the evaluation of the long term interaction between nitrate and chloroform pumping systems will require more data to be collected as part of routine monitoring. Slow development of hydraulic capture by the nitrate pumping system is consistent with and expected based on the relatively low permeability of the perched zone at the site. Definition of capture associated with the nitrate pumping system will also be influenced by the perched groundwater mound and the apparently anomalously low water level at TWN-7. Nitrate pumping is likely sufficient to eventually capture the entire nitrate plume upgradient of TW4-22 and TW4-24. Pumping during the current quarter was smaller than last quarter primarily due to the outage described in Section 5, but was within the range estimated for pre-pumping ('background') perched water flow through the nitrate plume. Because the pre-pumping flow calculations likely overestimate the new 'background' conditions caused by reduced recharge from the northern wildlife ponds, and because the average plume hydraulic conductivity estimate from the low end of the calculated range is likely to be more representative of actual conditions, current quarter nitrate pumping may exceed flow through the plume by a factor greater than 1.4. First quarter, 2015 nitrate concentrations at many of the wells within and adjacent to the nitrate plume were within 20% of the values reported during the previous quarter, suggesting that variations are within the range typical for sampling and analytical error. Changes in concentration greater than 20% occurred in MW-26, MW-27, TW4-16, TW4-19, TW4-20, TW4- 22, TW4-25, TWN-2, and TWN-18. The concentrations in wells MW-11, MW-25, and MW-32 remained non-detect. Of the wells showing changes in concentration greater than 20%, MW-26, TW4-19, and TW4-20 are chloroform pumping wells; and TW4-22, TW4-25 and TWN-2 are nitrate pumping wells. MW-27 is located adjacent to chloroform pumping well TWN-2; and TW4-16 is located adjacent to chloroform pumping well MW-26. Nitrate concentration fluctuations at pumping wells and adjacent wells likely result in part from the effects of pumping. Concentrations at TWN-18 are expected to be influenced by its location immediately up gradient of the nitrate plume .. 25 The nitrate concentration at TW4-25 increased from approximately 1 mg/L last quarter to approximately 14 mg/L this quarter, bringing it again within the nitrate plume boundary, and expanding the plume to the northeast. The nitrate concentrations in chloroform pumping wells MW-26, TW4-19, and TW4-20 increased from approximately 1.1 mg/L, 4.7 mg/L and 7.7 mg/L, respectively, to approximately 2.7 mg/L, 8.6 mg/L, and 9.8 mg/L, respectively. MW-27, located west ofTWN-2, and TWN-18, located north ofTWN-3, bound the nitrate plume to the west and north (See Figure 1-1 under Tab 1). In addition, the southernmost (downgradient) boundary of the plume remains between MW-30/MW-31 and MW-5/MW-11. Nitrate concentrations at MW-5 (adjacent to MW-11) and MW-11 have historically been low(< 1 mg/L) or non-detect for nitrate (See Table 5). MW-25, MW-26, MW-32, TW4-16, TW4-19, TW4-20, TWN-1, and TWN-4 bound the nitrate plume to the east. Although short-term fluctuations have occurred, nitrate concentrations in MW-30 and MW-31 have been relatively stable, demonstrating that plume migration is minimal or absent. Nitrate in MW-30 decreased from 16.2 mg/L to 14.9 mg/L and nitrate in MW-31 decreased from 20.9 mg/L to 18.7 mg/L. Based on the concentration data at MW-5, MW-11, MW-30, and MW-31, the nitrate plume is under control. Chloride has been relatively stable at MW -30 but is generally increasing at MW -31. The apparent increase in chloride and relatively stable nitrate at MW-31 suggests a natural attenuation process that is affecting nitrate but not chloride. A likely process that would degrade nitrate but leave chloride unaffected is reduction of nitrate by pyrite. The likelihood of this process in the perched zone is discussed in HGC, December 7 2012; Investigation of Pyrite in the Perched Zone, White Mesa Uranium Mill Site, Blanding, Utah. Nitrate mass removal by pumping and natural attenuation (expected to result primarily from pyrite oxidation/nitrate reduction) act to lower nitrate mass within the plume. Changes resulting from redistribution of nitrate within the plume are expected to result in both increases and decreases in concentrations at wells within the plume and therefore increases and decreases in mass estimates based on those concentrations, thus generating 'noise' in the mass estimates. Furthermore, because the sum of sampling and analytical error is typically about 20%, changes in the mass estimates from quarter to quarter of up to 20% could result from typical sampling and analytical error alone. Longer-term analyses of the mass estimates that minimize the impact of these quarter to quarter variations are expected to provide useful information on plume mass trends. Over the long term, nitrate mass estimates are expected to trend downward as a result of direct removal by pumping and through natural attenuation. As specified in the CAP, once eight quarters of data are collected (starting with the first quarter of 2013), a regression trend line is to be applied to the quarterly mass estimates and evaluated. The trend line is then to be updated quarterly and reevaluated as additional quarters of data are collected. As the previous quarter constituted the eighth quarter as specified in the CAP, the mass estimates were plotted, and a regression line was fitted to the data and evaluated. The regression line was updated this quarter as shown in Figure M.1 of Tab M. The fitted line shows a decreasing trend in the mass estimates. During the current quarter, a total of approximately 82.6 lb of nitrate was removed by the chloroform pumping wells and by nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN- 26 2. Of the 82.6 lb removed during the current quarter, approximately 67 lb, (or 81 %), was removed by the nitrate pumping wells. The baseline nitrate (nitrate+nitrite as N) plume mass calculated as specified in the CAP (based on second quarter, 2010 data) was approximately 43,700 lb. The mass estimate during the current quarter was calculated as 38,742 lb which was larger than the mass estimate during the previous quarter (34,370 lb) by 4,372 lb or 12.7 %. This difference results primarily from the increase in concentration at TW4-25 which increased the areal extent of the plume compared to last quarter. Nitrate concentrations outside the nitrate plume exceed 10 mg/L at a few locations: TW4-10 (15 mg/L), TW4-12 (19.2 mg/L), TW4-18 (11.7 mg/L), TW4-26 (14.4 mg/L), TW4-27 (26.5 mg/L), and TW4-28 (19 mg/L). All these wells are located southeast of the nitrate plume as defined in the CAP and all are separated from the plume by wells having nitrate concentrations that are either non-detect, or, if detected, are less than 10 mg/L. Concentrations at TW4-10, TW4-12, TW4-18, TW4-26, TW4-27 and TW4-28 are within 20% of their concentrations during the previous quarter. From the third quarter of 2013 through the second quarter of 2014, nitrate concentrations at TW4-10 and TW4-18 exceeded 10 mg/L, dropped below 10 mg/L in the third quarter of 2014, then increased above 10 mg/L last quarter. Elevated nitrate concentrations at these wells are associated with the chloroform plume, and both are within the capture zone of the chloroform pumping system. Elevated nitrate at TW4-12, TW4-26, TW4-27, and TW4-28 is likely related to former cattle ranching operations at the site. Increases in both nitrate and chloride concentrations at wells near the northern wildlife ponds (for example TW 4-18) were anticipated as a result of reduced dilution caused by cessation of water delivery to the northern wildlife ponds. However, decreasing nitrate concentrations at most wells in the vicinity of TW 4-18 from the first through third quarters of 2014 after a previously increasing trend (interrupted in the first quarter of 2014) suggest that conditions in this area have stabilized. Nitrate mass removal from the perched zone was increased substantially by the start-up of nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2 during the first quarter of 2013. Continued operation of these wells is therefore recommended. Pumping these wells, regardless of any short term fluctuations in concentrations detected at the wells, helps to reduce downgradient nitrate migration by removing nitrate mass and reducing average hydraulic gradients, thereby allowing natural attenuation to be more effective. Continued operation of the nitrate pumping system is expected to eventually reduce nitrate concentrations within the plume and to further reduce or halt downgradient nitrate migration. EFRI and its consultants have raised the issues and potential effects associated with cessation of water delivery to the northern wildlife ponds in March, 2012 during discussions with DRC in March 2012 and May 2013. While past recharge from the ponds has helped limit many constituent concentrations within the chloroform and nitrate plumes by dilution, the associated groundwater mounding has increased hydraulic gradients and contributed to plume migration. Since use of the northern wildlife ponds ceased in March 2012, the reduction in recharge and decay of the associated groundwater mound was expected to increase many constituent 27 concentrations within the plumes while reducing hydraulic gradients and rates of plume migration. The net impact of reduced wildlife pond recharge is expected to be beneficial even though it was also expected to result in temporarily higher concentrations until continued mass reduction via pumping and natural attenuation ultimately reduce concentrations. Temporary increases in nitrate concentrations are judged less important than reduced nitrate migration rates. The actual impacts of reduced recharge on concentrations and migration rates will be defined by continued monitoring. 8.0 ELECTRONIC DATA FILES AND FORMAT EFRI has provided to the Director an electronic copy of all laboratory results for groundwater quality monitoring conducted under the nitrate contaminant investigation during the quarter, in Comma Separated Values ("CSV") format. A copy of the transmittal e-mail is included under Tab L. 28 9.0 SIGNATURE AND CERTIFICATION This document was prepared by Energy Fuels Resources (USA) Inc. on May 20,2015. Energy Fuels Resources (USA) Inc. By: Scott Bakken Director, Permitting & Environmental Affairs 29 Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Scott Bakken Director, Permitting & Environmental Affairs Energy Fuels Resources (USA) Inc. 30 Tables Table 1 Summary of Well Sampling and Constituents for the Period Well Sampl~ Collect-ion Dnte Piezometer 01 2/18/2015 Piezometer 02 2/18/2015 Piezometer 03 2/18/2015 TWN-01 2/18/2015 TWN-02 2/18/2015 TWN-03 2/19/2015 TWN-04 2118/2015 TWN-07 2119/2015 TWN-07R 2/18/2015 TWN-18 2/18/2015 TW4-22 3/9/2015 1W4-24 3/9/2015 TW4-25 3/9/2015 TWN-60 2119/2015 TW4-60 3/17/2015 TWN-65 2/18/2015 Note: All wells were sampled for Nitrate and Chloride. TWN-60 is a Dl Field Blank. TWN-65 is a duplicate of TWN-01. TW4-60 is the chloroform program Dl Field Blank. Continuous.JM pumped well. Date of;_Lab Report 3/1112015 3/11/2015 3/11/2015 3/1112015 3/1112015 3/11/2015 3/11/2015 311112015 311112015 311112015 3/26/2015 3/26/2015 3/26/2015 3/11/2015 3/3112015 3/1112015 Table 2 Nitrate Mass Removal Per Well Per Quarter MW-4 MW·26 TW4-19 TW4-20 TW4-4 TW4-22 TW4-24 TW4-25 TWN..02 TW4..Ql TW4..Q2 TW4-11 Quarter Totals Quarter (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) (Jbs.) (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) Q3 2010 3.2 0.3 5.8 1.7 4.7 NA NA NA NA NA NA NA 15.69 Q4 2010 3.8 0.4 17.3 1.4 5.1 NA NA NA NA NA NA NA 27.97 Q1 2011 2.9 0.2 64.5 1.4 4.3 NA NA NA NA NA NA NA 73.30 Q22011 3.5 0.1 15.9 2.7 4.7 NA NA NA NA NA NA NA 27.01 Q3 2011 3.5 0.5 3.5 3.9 5.4 NA NA NA NA NA NA NA 16.82 Q4 2011 3.8 0.8 6.2 2.5 6.4 NA NA NA NA NA NA NA 19.71 Q1 2012 3.6 0.4 0.7 5.0 6.0 NA NA NA NA NA NA NA 15.86 Q2 2012 3.7 0.6 3.4 2.1 5.2 NA NA NA NA NA NA NA 15.03 Q3 2012 3.8 0.5 3.6 2.0 4.7 NA NA NA NA NA NA NA 14.67 Q4 2012 3.2 0.4 5.4 1.8 4.2 NA NA NA NA NA NA NA 14.92 Q1 2013 2.5 0.4 14.1 1.4 3.6 8.1 43.4 7.5 14.8 NA NA NA 95.73 Q2 2013 2.5 0.4 5.6 1.6 3.4 10.7 37.1 6.4 23.9 NA NA NA 91.71 Q3 2013 3.0 0.4 48.4 1.4 3.8 6.3 72.8 6.9 33.4 NA NA NA 176.53 Q4 2013 3.1 0.3 15.8 1.6 3.9 9.4 75.2 6.4 46.3 NA NA NA 162.07 Q1 2014 2.7 0.4 4.1 1.2 3.6 11.2 60.4 2.3 17.2 NA NA NA 103.14 Q2 2014 2.4 0.3 3.3 0.9 3.0 9.5 63.4 1.3 17.8 NA NA NA 101.87 Q3 2014 2.3 0.1 4.1 0.6 3.1 8.5 56.2 1.6 16.4 NA NA NA 92.99 Q4 2014 2.7 0.2 7.8 1.0 3.8 11.0 53.2 0.9 28.0 NA NA NA 108.57 QJ 2015 3.7 0.54 4.33 1.29 2.37 12.73 26.69 8.59 19.17 1.45 1.07 0.72 82.61 Well Totals (pounds) 59.93 7.42 233.90 35.70 81.28 87.45 488.31 41.98 216.98 1.45 1.07 0.72 1256.18 Table 3 Well Pumping Rates and Volumes Volume of Water Pumped Pumping Well Name During the Quarter (gals) Average Pump Rate (gpm) MW-4 76,454.3 4.60 MW-26 24,004.9 11.63 TW4-4 36,941.3 10.87 TW4-19 60,553.0 10.65 TW4-20 15,744.7 8.78 TW4-22 22,046.9 17.77 TW4-24 92,449.3 17.56 TW4-25 71,452.4 16.01 TWN-2 47,262.2 18.28 TW4-01 24,569.2 17.81 TW4-02 24,156.7 17.56 TW4-ll 9,898.7 17.92 Table 4 Table 4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped MW-4 MW-26 " -. - I I Total Total Total Pumped Total I Total ~otal Pumped Cone Cone Pumped Total Total Quarter Pumped (gal) .. Cone (mg/L) Cone (ug/L) (liters) Total (ug) (grams) (pounds) (gal) (mg/L) ~ {ug/L) (liters) Total (ug) (grams) (pounds) Total Gallons pumped for Total the quarter Total pumped Total grams/453. ] Calculations from the Concentration Concentration gallons/3.785 Concentration ug/1000000 592 to 1. II and Data Flow Meter from the in mgfLX1000 to to conver to in ugll X total to convert to convert to Origination data analytical data convert to ug/L, liters liters grams I pounds = ~ Q3 2.010 79859.1 4.8 4800 302.2.66.7 145088012.9 1450.9 3.2.0 63850.0 0.6 600 2.41672..3 145003350 145 0.32. Q42.010 90042..2. 5 5000 340809.7 1704048635 1704.0 3.76 60180.0 0.7 700 2.27781.3 159446910 159 0.35 Ql2.011 762.47.6 4.6 4600 288597.2. 132.7546964 132.7.5 2,93 55130.0 0.5 500 208667.1 10433352.5 104 0.23 Q2 2.011 85849.3 4.9 4900 32.4939.6 1592.2.04042 1592.2 3.51 55800.6 0.3 300 211205.3 63361581 63 0.14 03.2011 8532.7,7 4.9 4900 322965.3 1582.530188 1582.5 3.49 65618.0 0.9 900 2.48364.1 223527717 224 0.49 Q4 2011 89735.0 5.1 5100 339647.0 1732199573 1732..2 3.82 50191.3 2 2000 189974.1 379948141 380 0.84 Q12012 90376.4 4.8 4800 342074.7 1641958435 1642.0 3.62 31440.1 1.7 1700 119000.8 202301323 202 0,45 Q2 2012. 90916.5 4.9 4900 344118.8 1686181940 1686.2 3.72 26701.2 2.5 2500 101064.1 252660294 253 0.56 Q3 2012 91607.0 5 5000 346732.5 1733662475 1733.7 3.82. 2.5246.0 2.6 2600 95556.1 248445886 248 0.55 Q4 2012 78840.0 4.8 4800 298409.4 1432365120 1432.4 3.16 30797.0 1.46 1460 116566.6 170187302 170 0.38 Q12013 62.943.7 4.78 4780 238241.9 1138796304 1138.8 2.51 22650.7 2.27 2270 85732.9 194613682 195 0.43 Q2 2013 71187.3 4.22 42.2.0 269443.9 1137053387 1137.1 2.51 25343.4 2.11 2110 95924.8 202401263 202 0.45 Q3 2013 72898.8 4.89 4890 275922.0 1349258375 1349.3 2..97 25763.0 1.98 1980 97513.0 193075651 193 0.43 Q42013 70340.4 5.25 5250 266238.4 1397751674 1397.8 3.08 24207.6 1.38 1380 91625.8 126443557 126 0.2.8 Q12014 69833.8 4.7 4700 2.64320.9 1242.308385 1242.3 2.74 23263.1 2.12 2120 88050.8 186667767 187 0.41 Q2 2014 71934.9 4.08 4080 272273.6 1110876274 1110,9 2.45 23757.5 1.42 1420 89922.1 127689435 128 0.28 Q3 2014 74788.2 3.7 3700 283073.3 1047371347 1047.4 2.31 24062.4 0.7 700 91076.2 63753329 64 0.14 Q4 2014 63093.0 5.07 5070 238807.0 1210751515 1210.8 2.67 21875.8 0.934 934 82799.9 77335109 77 0.17 Ql2015 76454.3 5.75 5750 289379.5 1663932272. 1663.9 3.67 24004.9 2..68 2680 90858.5 243500905 2.44 0.54 Totals Since Q3 2010 14922.75.15 59.93 679882,6 7.42 Highlighted cells are the total for the current quarter Table 4 Table 4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped TW4-19 ~ TW4-20 " Total Pumped Cone Cone Total Pumped Total Total !Total Pumped Cone Cone Total Pumped Total Total Quarter (gal) (mg/L) (ug/L) (liters) Total (ug) (grams) (pounds) (gal) (mg/L) I (ug/L) (liters) Total (ug) (grams) (pounds) ~ I I I ~ I. I I Calculations : ~ I and Data I' Origination ' I 03 2010 116899.2 5.9 5900 442463.5 2.611E+09 2611 5.76 39098.3 5.3 5300 147987.1 784331447 784 1.73 04 2010 767970.5 2.7 2700 2906768,3 7.848E+09 7848 17.30 36752.5 4.6 4600 139108.2 639897778 640 1.41 012011 454607.9 17 17000 1720690.9 2.925E+10 29252 64,49 37187.5 4.4 4400 140754.7 619320625 619 1.37 02 2011 159238.9 12 12000 602719_2 7.233E+09 7233 15.95 67907.7 4.8 4800 257030.6 1.234E+09 1234 2.72 03 2011 141542.6 3 3000 535738.7 1.607E+09 1607 3.54 72311.2 6.5 6500 273697.9 1.779E+09 1779 3.92 04 2011 147647.2 5 5000 558844.7 2.794E+09 2794 6.16 72089.3 4.2 4200 272858.0 1.146E+09 1146 2.53 012012 148747.0 0.6 600 563007.4 337804437 338 0.74 76306.0 7.9 7900 288818.2 2.282E+09 2282 5.03 02 2012 172082.0 2.4 2400 651330.5 1.563E+09 1563 3.45 22956.4 11 11000 86890.1 955790963 956 2.11 03 2012 171345.0 2.5 2500 648540.8 1.621E+09 1621 3.57 22025.0 10.8 10800 83364.6 900337950 900 1.98 04 2012 156653.0 4.1 4100 592931.6 2.431E+09 2431 5.36 20114.0 11 11000 76131.5 837446390 837 1.85 012013 210908.0 7.99 7990 798286.8 6.378E+09 6378 14.06 18177.0 9.07 9070 68799.9 624015501 624 1.38 02 2013 226224.0 2.95 2950 856257.8 2.526E+09 2526 5.57 20252.4 9.76 9760 76655.3 748156060 748 1.65 03 2013 329460.1 17.6 17600 1247006.5 2.195E+10 21947 48.39 19731.0 8.65 8650 74681.8 645997873 646 1.42 042013 403974.0 4.7 4700 1529041.6 7.186E+09 7186 15.84 19280.2 9.64 9640 72975.6 703484369 703 1.55 012014 304851.0 1.62 1620 1153861.0 1.869E+09 1869 4.12 18781.6 7.56 7560 71088.4 537427971 537 1.18 02 2014 297660.0 1.34 1340 1126643.1 1.51E+09 1510 3.33 18462.4 5.95 5950 69880.2 415787095 416 0.92 03 2014 309742.0 1.6 1600 1172373.5 1.876E+09 1876 4.14 17237.9 4.3 4300 65245.5 280555441 281 0.62 Q4 2014 198331,0 4.72 4720 750682.8 3.543E+09 3543 7.81 16341.8 7.67 7670 61853.7 474417979 474 1.05 012015 60553.0 8.56 8560 229193.1 1.962E+09 1962 4.33 15744.7 9.8 9800 59593.7 584018157 584 I 1.29 Totals Since Q3 2010 4778436.4 233.90 630756.9 35.70 Highlighted cells are the total for the current quarter Table4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped TW4-4 TW4-ZZ " . Total Total I Total Total Pumped Cone Cone Pumped Total Total Pumped Cone Cone Pumped Total Total Quarter (gal) (m!Jil) (u!Jil) (liters) Total (ug) (grams) (pounds) (gal) (mg/L) (ugll) (liters) Total (ug) (grams) (pounds) I II ! I Calculations I II I and Data I Origination Q3 2010 76916.8 7.30 7300.00 291130.1 2.1E+09 2125.25 4.69 NA NA NA NA NA NA NA Q4 2010 86872.1 7.10 7100.00 328810.9 2.3E+09 2334.56 5.15 NA NA NA NA NA NA NA Q12011 73360.0 7.00 7000.00 277667.6 1.9E+09 1943.67 4.29 NA NA NA NA NA NA NA Q2 2011 80334.6 7.00 7000.00 304066.5 2.1E+09 2128.47 4.69 NA NA NA NA NA NA NA Q3 2011 97535.0 6.60 6600.00 369170.0 2.4E+09 2436.52 5.37 NA NA NA NA NA NA NA Q4 2011 109043.5 7.00 7000.00 412729.6 2.9E+09 2889.11 6.37 NA NA NA NA NA NA NA Q12012 101616.8 7.10 7100.00 384619.6 2.7E+09 2730.80 6.02 NA NA NA NA NA NA NA Q2 2012 87759.1 7.10 7100.00 332168.2 2.4E+09 2358.39 5.20 NA NA NA NA NA NA NA Q3 2012 80006.0 7.10 7100.00 302822.7 2.2E+09 2150.04 4.74 NA NA NA NA NA NA NA Q4 2012 71596.0 7.00 7000.00 270990.9 1.9E+09 1896.94 4.18 NA NA NA NA NA NA NA Q12013 58716.8 7.36 7360.00 222243,1 1.6E+09 1635.71 3.61 16677.4 58.0 58000.0 63124.0 3661189622.0 3661.2 8.07 Q2 2013 65603.4 6.30 6300.00 248308.9 1.6E+09 1564.35 3.45 25523.2 50.2 50200.0 96605.3 4849586662.4 4849.6 10.69 Q3 2013 63515.4 7.22 7220.00 240405.8 1.7E+09 1735.73 3.83 25592.9 29.7 29700.0 96869.1 2877013057.1 2877.0 6.34 Q4 2013 60233.6 7.84 7840.00 227984.2 1.8E+09 1787.40 3.94 24952.2 45,2 45200.0 94444.1 4268872280.4 4268.9 9.41 Q12014 58992.9 7.28 7280.00 223288.1 1.6E+09 1625.54 3.58 24532.0 54.6 54600.0 92853.6 5069807652.0 5069.8 11.18 Q2 2014 60235.3 5.91 5910.00 227990.6 1.3E+09 1347.42 2.97 24193.9 47.2 47200.0 91573.9 4322288622.8 4322.3 9.53 Q3 2014 69229.4 5.30 5300.00 262033.3 1.4E+09 1388.78 3.06 24610.9 41.5 41500.0 93152.3 3865818644.8 3865.8 8.52 Q4 2014 64422.6 7.02 7020.00 243839.5 1.7E+09 1711.75 3.77 23956.9 54.9 54900.0 90676.9 4978159970.9 4978.2 10.97 Q12015 36941.3 7.70 7700.00 139822.8 1.1E+09 1076.64 2.37 22046.9 69.2 69200.0 83447.5 '-5774568141.8 5774.6 12.73 Totals Since Q3 2010 1402930.6 81.28 212086.3 87.45 Highlighted cells are the total for the current quarter Table4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped lW4-24 lW4-25 7· I I Total Total Total Total Pumped Cone Cone Pumped Total Total Pumped Cone Cone Pumped Total Total Quarter (gal) (mgll) 11 (ugll) (liters) Total (ug) (grams) (pounds) (gal) (mgfl) (ugll) (liters) Total (ug) (grams) (pounds) I I I Calculations and Data I Origination l I Q3 2010 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q4 2010 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q12011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q2 2011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q3 2011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q4 2011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q12012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q2 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q3 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q4 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q12013 144842.6 35.9 35900.0 548229.2 19681429751.9 19681.4 43,39 99369.9 9.0 9000.0 376115.1 3385035643.5 3385.0 7.46 Q2 2013 187509.3 23.7 23700.0 709722.7 16820428001.9 16820.4 37.08 147310.4 52 5240.0 557569.9 2921666087.4 2921.7 6.44 Q3 2013 267703.5 32.6 32600.0 1013257.7 33032202568.5 33032.2 72.82 145840.9 5.69 5690.0 552007.8 3140924419.0 3140.9 6.92 I Q4 2013 260555.3 34.6 34600.0 986201.8 34122582643.3 34122.6 75,23 126576.5 6.10 6100.0 479092.1 2922461520.3 2922.5 6.44 Q12014 229063.9 31.6 31600.0 867006.9 27397416823.4 27397.4 60.40 129979.2 2.16 2160.0 491971.3 1062657947.5 1062.7 2.34 Q2 2014 216984.1 35.0 35000.0 821284.8 28744968647.5 28745.0 63.37 124829.8 1.21 1210.0 472480.8 571701759.5 571.7 1.26 Q3 2014 213652.5 31.5 31500.0 808674.7 254 73253443.8 25473.3 56.16 119663.9 1.60 1600.0 452927.9 724684578.4 724.7 1.60 Q4 2014 178468.7 35.7 35700.0 675504.0 24115493853.2 24115.5 53.17 107416.1 1.03 1030.0 406569.9 418767036.7 418.8 0.92 Q12015 92449.3 34.6 34600.0 349920.6 12107252777.3 12107.3 26.69 71452.4 14.40 14400.0 270447.3 3894441609.6 3894.4 8.59 Totals Since Q3 2010 1791229.2 488.31 1072439.1 41.98 Highlighted cells are the total for the current quarter Table 4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped lWN-oz 1W4-01 --I - I I I Total Total Total Total Pumped Cone Cone Pumped Total Total Pumped Cone Cone Pumped Total Total Quarter (gal) (mgll) (ugfl) (liters) Total (ug) (grams) (pounds) (gal) (mgfl) (ugfl) (liters) Total (ug) (grams) (pounds) I' ' Calculations I and Data I. l Origination - 03 2010 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 04 2010 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q12011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q2 2011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 03 2011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 04 2011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 012012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q2 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q3 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q4 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA I Q12013 31009.4 57.3 57300.0 117370.6 6725334176.7 6725.3 14.83 NA NA NA NA NA NA NA I Q2 2013 49579.3 57.7 57700.0 187657.7 10827846433.9 10827.8 23.87 NA NA NA NA NA NA NA I Q3 2013 50036.5 80.0 80000.0 189388.2 15151052200.0 15151.1 33.40 NA NA NA NA NA NA NA Q4 2013 49979.9 111.0 111000.0 189173.9 20998305286.5 20998.3 46.29 NA NA NA NA NA NA NA Q12014 48320.4 42.6 42600.0 182892.7 7791229616.4 7791.2 17.18 NA NA NA NA NA NA NA Q2 2014 47611.9 44.7 44700.0 180211.0 8055433555.1 8055.4 17.76 NA NA NA NA NA NA NA Q3 2014 46927.2 42.0 42000.0 177619.5 7460016984.0 7460.0 16.45 NA NA NA NA NA NA NA Q4 2014 47585.6 70.6 70600.0 180111.5 12715871617.6 12715.9 28.03 NA NA NA NA NA NA NA 012015 47262.2 48.6 48600.0 178887.4 8693928952.2 8693.9 19.17 24569.2 7.1 7060.0 92994.4 656540619.3 656 5 1.45 Totals Since Q3 2010 418312.4 216.98 24569.2 1.45 Highlighted tells are the total for the current quarter Highlighted tells are the total for the current quarter Table 4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped TW4-02 ·-· TW4-ll ] Total ,, Removed Total Total Total Total by All Pumped Cone Cone Pumped Total Total Pumped Cone Cone Pumped Total Total Wells Quarter (gal) (mg/L) (ugfL) (liters) Total (ug) (grams) (pounds) (gal) (mgfL) (ugfL) (liters) Total (ug) (grams) (pounds) (pounds) I l . I. I Calculations 1: and Data ' Origination Q3 2010 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 15_69 Q4 2010 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 27.97 I Q12011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 73.30 Q2 2011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 27.01 I Q3 2011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 16.82 Q4 2011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 19.71 I Q12012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 15.86 Q2 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 15.03 Q3 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 14.67 I Q4 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 14.92 Q12013 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 95.73 I Q2 2013 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 91.71 I Q3 2013 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 176.53 Q4 2013 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 162.07 Q12014 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 103.14 Q2 2014 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 101.87 Q3 2014 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 92.99 Q4 2014 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 108.57 Q12015 24156.7 ~.3 5320.0 91433.1 486424142.5 486.4 1.07 9898.7 8.7 8720.0 37466.6 326708573.2 326.7 0.72 82.61 ---- Totals Since Q3 2010 24156.7 1.07 9898.7 0.72 1256.18 Highlighted cells are the total for the current quarter Highlighted cells are the total for the current quarter Q2 L00atio.n 20J,O MW..SO 15.8 _M W'-3J 22.5 ~f\\1!:5 ND MW~l '"" ND ND =Not detected NS = Not Sampled QS. "Q4 QJ 20t0 Z{>l,O 2_011 15 16 16 21 20 21 NS 0.2 NS ND ND ND TableS Nitrate Data Over Time for MW-30. MW-31. MW-5. and MW-11 ' Q2' w Q~ Ql Q2 Q3· Q4 ;Ql ~2 P@ Q4 Ql ~2 Q3· Q4. Ql f!- 2011 2011 20LL W 12 2012 201 2~ 20'12 2{)13 L 20 1 ~ 2!ll.l.3 2Ql-3; 20)4 20Lil 20J-E~i_, 2'014 10l5 17 16 16 17 16 17 18.5 21.4 18.8 17.6 19.5 18.4 19.4 16.8 16.2 14.9 22 21 21 21 20 21 23.6 19.3 23.8 21.7 23.9 20.6 23.1 18.9 20.9 18.7 0.2 NS 0.2 NS 0.1 NS ND NS ND NS 0.279 NS ND NS 0.21 NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND TABLE 6 Slug Test Results (Using KGS Solution and Automatically Logged Data) Well K lcm/s) MW-30 1.0E-04 MW-31 7.1E-05 TW4-22 1.3E-04 TW4-24 1.6E-04 TW4-25 5.8E-05 TWN-2 1.5E-05 TWN-3 8.6E-06 Average 1 Average2 Average 3 Average 4 Notes: Average 1 = arithemetic average of all wells Average 2 =geometric average of all wells K JftldaY} 0.28 0.20 0.36 0.45 0.16 0.042 0.024 0.22 0.15 0.32 0.31 Average 3 = arithemetic average of MW-30, MW-31, TW4-22, and TW4-24 Average 4 =geometric average of MW-30, MW-31, TW4-22, and TW4-24 cmls = centimeters per second ft!day = feet per day K = hydraulic conductivity KGS = KGS Unconfined Slug Test Solution in Aqtesolve ™. S:\Environmentai\UnWhiteMesaMiii\Required Reports\Nitrate Quarterly Report\2015 01\FiowCalcs-Tables 6-7-8: Table 6 TABLE 7 Pre-Pumping Saturated Thicknesses Depth to Depth to Water Saturated Thickness Well Brushy Basin Fourth Quarter, 2012 Above Brushy Basin (ft) (ft) (ft) TW4-22 112 53 58 TW4-24 110 55 55 Notes: ft =feet S:\Environmentai\UT\WhiteMesaMiii\Required Reports\Nitrate Quarterly Report\2015 Q1\FiowCalcs-Tables 6-7-8: Table 7 TABLE 8 Pre-Pumping Hydraulic Gradients and Flow Calculations Pathline Boundaries Path Length Head Change Hydraulic Gradient (ft) (ft) (ftlft) TW4-25 to MW-31 2060 48 0.023 TWN-2 to MW-30 2450 67 0.027 average 0.025 1 min flow (gpm) 1.31 2 max flow (gpm) 2.79 Notes: ft =feet ft!ft = feet per foot gpm = gallons per minute 1 assumes width = 1 ,200 ft; saturated thickness = 56 ft; K = 0.15 ft/day; and gradient = 0.025 ft/ft 2 assumes width = 1 ,200 ft; saturated thickness = 56 ft; K = 0.32 ft/day; and gradient = 0.025 ft/ft S:\Environmentai\UT\WhitaMesaMiii\Required Reports\Nitrate Quarterly Report\2015 Q1\FiowCalcs-Tables 6-7-8: Table 8 INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and Field Data Worksheets Tab C Kriged Current Quarter Groundwater Contour Map, Capture Zone Map, Capture Zone Details Map, and Weekly, Monthly and Quarterly Depth to Water Data Tab D Kriged Previous Quarter Groundwater Contour Map Tab E Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells Tab F Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Tab G Laboratory Analytical Reports Tab H Quality Assurance and Data Validation Tables H-1 Field Data QA/QC Evaluation H-2 Holding Time Evaluation H-3 Analytical Method Check H-4 Reporting Limit Evaluation H-5 QAJQC Evaluation for Sample Duplicates H-6 QC Control Limits for Analyses and Blanks H-7 Receipt Temperature Evaluation H-8 Rinsate Evaluation Tab I Kriged Current Quarter Isoconcentration Maps Tab J Analyte Concentration Data Over Time Tab K Concentration Trend Graphs Tab L CSV Transmittal Letter Tab M Residual Mass Estimate Analysis Figures and Tables Tab A Site Plan and Perched Well Locations White Mesa Site TW4-37 • temporary perched monitoring well installed March, 2015 TW4-19 EB perched chloroform or nitrate pumping well MW-5 • perched monitoring well TW4·12 0 temporary perched monitoring well TWN-7 ~ temporary perched nitrate monitoring well PIEZ-1 ~ perched piezometer TW4-35 temporary perched monitoring well ~ installed May, 2014 RUIN SPRING ~ seep or spring HYDRO GEO CHEM,INC. WHITE MESA SITE PLAN SHOWING LOCATIONS OF PERCHED WELLS AND PIEZOMETERS REFERENCE I FIGURE H :/718000/may15/Uwelloc0315_rev .srf A-1 TabB Order of Sampling and Field Data Worksheets Nitrate Mg/L Previous c Nitrate Samples Name Qrt. Date/Purge sample TWN-7 0.968 TWN-4 1.44 TWN-1 1.46 TWN-18 1.47 TWN-3 19.1 TWN-2 70.6 Duplicate of Rinsate 'fw,l)-o\ 01 Sample -f'.,..V -r..O Plez 1 5.75 Piez 2 0.755 Piez 3 1.74 2./.1'1 J I~ 07"3_f.) 1~18'/tS rzse:. z../Wit:, 132-S VlstJL"'l iYDi z.li'IILS o-7'15 17./1~/15 e>g-z..s '1./ Iff/IS l3'Z.S 2/1~/15 \It)/ l.z.Jiq/LI':; 0/11) '2./lgJ !5 b851 "Z/IY l5 0&35 2118/!.5 ozY.S Nitrate Order 1st Quarter 2015 Depth Total Depth 105 125.7 112.5 145 96 96 Name TWN-7R TWN-4R TWN-lR TWN-lBR TWN-3R TWN-2R Samplers: ( Rlnsate Samples Date Sample 17/'1'/~ 1157 MiD-Gcaundwater Discharge Permit Groundwater Monltoring Quality Assurance Plan IQAP) Date: 06-06-12 Rev. 7. 2 -Errata AITACBMENT 1-2 WHITE MESA URANIUM MILL FolELDDATA WORKSHEET FOR GROUNDWATER "'j See instruction Description of Sampling Event I 1 ~,. Q-.. ... r ·h:r N •+rc:~.fe zD 1.5 Sampler Name Location (well name): IL.--I.Pi-!.l .::::.e"L.::::.....-.....;0~1 -----------' and initials: 1 -r:nn~r Ho iJ,J,.,,::~J.rH Field Sample ID Date and Time for Purging ._I _'2..~1 :..:.18~1..:-z....::;o~LS~----_. Well Purging Equip Used: [QJ purnp or ~~ bailer and Sampling (if different)!._ :..::rJ~/..t...;f!l'-----------1 Well Pump (if other than Bem1et) .... 1 -~-'/-~~-------' Purging Method Used: [QJ2 casings [QJ3 casings Sampling Event I O .... o..r ted.<i A) dr ... +e: Prev. Well Sampled in Saillpling Event I f, ~~-0~ pH Buffer 7 n ,_1___,7"'-.o ____ __, Specific Conductance ,_I ..;.J,;;,.tlo;;..;o:.._ ___ _.l J!MHOS/ em Depth to Water Before Purging 164 .S& Weather Cond. Tinle l o ~ I Gal. Purged I 0 Conductance I '2.i2~ I pH I g,£}3 Temp. ac I 11.20 I Redox Potential Eh (mV) I i ~·:) I Turbidity (NTU) I 0 I Time I I Gal. Purged I Conductance I I pH I Temp. "C I I Redox Potential Eh. (m V) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater I I I I pH Buffer 4.0 L..j,O Well Depth(O.Olft): ._I _o ____ _j Casing Volume (V) 4" Well:~-0----11(.653h) 3" Well:_ o (.3G7h) Ext'l Amb. Temp. •c (prior sampling event)l._3...;..~ __ __, Time I I GaL Purged I I Conductance I I pHI I Temp. oc I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Time I I Gal. Purged I I Conductance I I pHI I Temp. "C I I Redox Potential Eh (mV) I I Turbidity (NTU) I I 1 of2 Capturx· COMPATIBLE WITH~.ti:r--FIINCTIONAUTY Mill-Gr.oundwater Dis~harge Permit Groundwater Monitoring Quality Assurance Plan IO,AP) ( Date. 06-06-12 Rev. 7.2-Errata Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flov.· Rate (Q). in gpm. Time to evacuate two casing volumes (2V) S/60 = I () T=2V/Q=I 0 I Nnmber of casing volumes evacuated (if other than two) D If well eYacuated to dryness, number of gallons e,·acuated 0 Name of Certified Analytical Labomtory if Other Than Energy Labs ,AWi\L Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients Cil D 100m! D ~ H2S04 s D Heavy Metals 0 0 250m! 0 0 HN03 0 0 AJJ Other Non Radiologies 0 0 250m! D 0 No Preserv_ 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 D l>thcr (specify) Iii 0 Sample volume 0 Ul 0 ~ C.\,lor,je-If preservative is used, spe<:ify Type and Quantity of Preservative· ~ Final Depth j (;)-l , f> 2-Sample Time ! :Comment i See instruction ·' Arr 1 1le~ on srte (;\.+-085;2 S.~rv1p1e~ 6G'.,JeJ "'+ og57 -ro..nn~r o.l\~ GMr111 pr~<!ll.J.--f~ Colle<-+ .5..:onp1e~. wo..+e.r w~ IY\C.·.)+~ Glct\( buJ h"~ Sal")~ wocA 1/~ r.._rfn.:.lr:.-j Aotfll~ Le.H $.i+~ o.t DGJOO 1-----------'IDo not touch this cell (SheetName) :; White Mesa Mill Field Data Worksheet for Groundwater A 2 of2 capturx· COM.ATIOLE WITH/'-...-..ori:r-FUNCTIONALITY Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I l !>T G\Ao..f" t-er N-1-l-rotfc: zo15 See instruction Location (well name): L]_P..:...':...;e:..:'Z.::::.---=-0-=7.=------------J Sampler N arne and initials: ] -rAnna HoJJ,'J~-:1 1-r/J Field Sample ID Date and Time for Purging ]L__"2_./c...;-l'""'~'-'-/-='Z;;.::O~IS..l-------' and Sampling (if different) /lllfJr Well Purging Equip Used: [g]pump or IT[] bailer Well Pump (if other than Bennet) ...VIA Purging Method Used: [g]2 casings [gJ3 casings Sampling Event Qu.o.d:-e.rl~ A)J,.o...te.. Prev. Well Sampled in Sampling Event l jwA) _, O 2.... pH Buffer 7.0 pH Buffer 4.0 LJ.O Specific Conductance ._I _lo_o_o ____ _.] [.tMHOS/ em Well Depth(O.Olft): ._I ..;;...0 ____ __, Depth to Water Before Purging ] ~ b, 55.5 Casing Volume (V) 4" Wcll:~_o ___ -ll(.653h) 3" Well:_ 0 _(.367h) Weather Cond. Ext'l Amb . Temp. oc (prior sampling event),_] 2_0 __ __, Time I os3.3 I Gal. Purged I 0 I Time I I Gal. Purged I I Conductance 11'10 I pH I eo.r67 I Conductance I I pHI I Temp. oc I r~.-.sq I Temp. oc I I Redox Potential Eh (m V) I 2'f~ I Redox Potential Eh (m V) I I Turbidity (NTU) I Q I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (mV) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q}, in gprm . S/60 = I 6 Time to evacuate two ca·sing volumes (2V) T=2V/Q= I D I Number of casing volumes evacuated (if other than two) l o If well evacuated to dryness, number of gallons evacuated I o Name of Certified Analytical Laboratory if Other Than Energy Labs ~..1 ....;.A_VJ'--A.;...L ______ _. Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) VOCs D D 3x40 ml Nutrients ~ D IOOml Heavy Metals D D 250m! All Other Non Radiologies D D 250ml Gross Alpha D D 1,000 ml Other (specify) ~ D Sample volume Gh 1or;Je. Final Depth I 37, L J Sample Time Comment A n·;~e~ on ~it~ o.t o~ J"Mt:f" Mlj. 6-o.((ifl pt'~ed­ ~~r1f)~ bo._;)ea ~t O~,S Wti\ter w~s MDS~ Le& sli-~ (At o83~ Piez-02 02-18-2015 !Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater y N y D D HCL D D ~ H2S04 13 D D HN03 D D D No Preserv. D D D HN03 D D 1!9 ~ If preservative is used, specify Type and Quantity of Preservative: ·h co llecf--.$Ml1pJ~. c. lear See instruction N D D D D D M 2 of 2 ~ .. , : Mill-Grotr.ldwater ~charge Permit ( Date: 06-()6-12 Rev. 7.2-Errata Groundwater Monitoring Quafity Assurance Plan (QA.P) ATTACHMENT 1-2 · :~~,,..u..L. WlDTE MESA URANIUM MILL See instruction FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I \ ~'T Qv,"'r f~l"' IV ·h-.,+e ZD l5 Location (well name): L--1 --~.P~1=e."t.!!L-:....D~)~--------__. Sampler Name and initials: I ·~V!nc=r Hl!JJ,Jq1/IH Field Sample ID Date and Time for Purging l._-=l.:.L/-LI.!l&.~.-/.z=.2~0..:..1 S..l------' WellPurgingEquip Used: IQ]pump or ~bailer and Sampling (if different) IL.,;.v.:=LJVAo.-_______ __.j Well Pwnp (if other than BenneL) l.._-v..;..:....:-"-'.=--------' Purging Method Used: [QJ2 casings @]3 casings Sampling Event j QV\o..-}~rlj A.l l.fr.,t, Prev. Well Sampled in SamplingEvent I =ft.tht) 'Rc:z.-DZ pH Buffer 7.0 ._! ___,_/.:...;:.0'-------' pH Buffer 4 0 Specific Conductance ._I -',_oo-'o;..._ ___ _.lflMElOSf em Well Depth(O.Olft): ._I ....;.o ____ __. Depth to Water Before Purging I L!'1 -g ') casing Volwnc (V) 4" weu :r_o ___ --ij<-65311) 3" Well:_ o _ (.36711) Weather Cond. Ext'! Am b. Temp. •c (prior sampling event}._l ..;;.3 _0 __ _. Time I ol643 I GaL Purged I 6 I Time I I Gal. Purged I I Conductance I 211.,~ I pH I l1.2.3 I Conductance I I pHI I Temp_ oc I j·~.-2.~ I Temp. °C I I Redox Potential Eh (mV) I 1 '1~ I Redox Potential Eh (m V) I I Turbidity (NTU) I 0 I Turbidity (NTIJ) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. °C I. l Temp. oc I I Redox Potential Eb (mV) I I Redox Potential Eh (mV) I I Turbidity (NTIJ) I I Turbidity {NTU) I I White MeSil Mill Field Data Worksheet for Groundwater-.A 1 of2 capturx-COWPHIILE WITN/"U."'Ii;--FUNCTIONALITY Mill-Groundw•ter Discharge P!!rmit ( Date. 01>-06-12 Rev. 7 2 -Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged D galfon(s) Pumping Rate Calculation Flow Rate (Q). in gpm, S/60 = I 0 Time to evacuate two casing volumes (2V) T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) I D If well evacuated to dryness, number of gallons evacuated D Name of Certified Analytical Laboratory if Other Than Energy Labs [}.!..~....!.'A..:..:L=-------~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if oti1er than as Prcservalive Type y N specified below) VOCs 0 0 3x40 ml Nutrients Iii 0 lOOml Hea-vy Metals 0 0 250ml All Other Non Radiologies 0 0 250 rnl Gross Alpha 0 0 l,OOOml OU1cr (specify) m 0 Sample volume C..h \oc ' Je rinal Depth I 4 -~ ~ Sample Time :.Comment -( ... 1\ner (}.flJ.. G-o.rcin -pre!>.dl f 1 Pu·r;veJ.. on s.r+e u.+ 0 ~'iC SP'-t'Y\ p'l e~ bo-; ) e a "'~ ,:--g•-1.1) wa--+er 1.\).:;.._s. rno~t~ Le. ft s I +-e. ((T-0 fS'18' L....-_________ __.IDo not touch this cell (SheetName) WhiteMes;~Mill Field Date; Workshe!!t for Groundwater y 0 0 0 0 0 0 N 0 IE 0 D 0 12!1 y HC'L 0 H2S04 fa HN03 0 No Preserv. 0 HN03 0 0 If preservative is used, spccil:)' Type and Quantity of Preservative: See instruction > +..:. CD )/e c+ ..:Yo117p 7~ ckar N 0 0 0 0 0 119 Mm -Groundw~ter Discharge Permit / \. Date; 06-06-12 Rev 7 _ 2 -Errata Groundwater ~onitoring Quality Assurant@ Plan (QAP) I i l t . ; 1 ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I I ~T O.~N>-der A:Ji+r-d~ z.oi:S • Sec insbUctioo Sampler Name Location (well name): I -rw.N-01 and initials: I ~""~' Hoil·f!j 1!11 Field Sample ID Date and Time for Purging ~-.I _ ... ::;._...:.../..:..:.l~<..l./_,z=-=o:..;,:'!:.==-----___. Well Purging Equip Used: ~pump or [gJ bailer and Sampling (if different) I~,.;M;..;:~~;tl~---------~ Well Pump (if other than Bennet) I Gr.JMI ·to? Purging Method Used: 002 casings IQJJ casings Sampling Event I Q~r·tef b N ~h~tc Prev. Well Sampled in Sampling E\'ent l ·==(v::n:,r:::"07 · -rw;J-Oif 'Tw,V·O~ pH Buffer 7.0 17.0 pH Buffer 4.0 j .o Specific Conductance ._I _:.I_::;_Do:...:o'-------'IJ-1 ifHOS' em Well Depth(O.Olft): I li'2-~0 Depth to Water Before Purging I (::P. ~& Casing Volume (V) 4" Well:' ;53 10 ,(.653b) 3" Well :~__ o.;;..._ __ _J_(.367h) Weather Cond. Ext'l Am b. Temp. •c (prior sampling event)._! 'f.._' __ ___. Time I r~tz I Gal. Purged I 5~ I Time 1 1'32..~ I Gal. Purged I l,f: I Conductance I ~:1~ I pH I b .1S I Conductance I ~"'I I pH I b..7b I Temp. °C I \S .O'J I Temp. °C I 1S.0'1 I Redox Potential Eh (m V) I I~F ·--, Redox Potential Eh (mV) 1 l"'h I Turbidity (NTU) I n I Turbidity {NTU) I O I Time I 1'3-zq I Gal. Purged I 77 I Time I P ZS I Gal. Purged I g~ I Conductance I ~~~ I pH I ~.'"16 I Conductance I 8:>~ I pHI 6 .78' I Temp. oc I \?.Ol:. I Temp. oc II ~ 07 _j Redox Potential Eh (mV) I ~~~ I Redox Potential Eh (m V) I l j ;i I Turbidity (NTU) I 0 I Turbidity (NTU) l o I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Capturx· COIOPATIILE WIT!l_...dn.,.k--FUNCTIONALITY Mill-Groundwater Discharge Permit Date 06-06-12 Rev. 7.2 -Err.lta Groundwater ~onitoring Quality A••urance Plan IQAP) Volmne of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q). in g,pm. S/60 = I 11.0 Number of casing volumes evacuated (if oilier than lwo) Time to evacuate two casing volumes (2V) T=2VIQ= I f>,l2 "] I o If well e\'acuated to dryness, number of gallons evacuated ._I _C: ---....J Name of Cenified Analytical Laboratory if Other Timn Energy Labs IL...;....A;_W...:..i\:..::L,__ ____ _. Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if oilier than as Preservative Type VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specify) C.h\or ;de ~inal Depth I [07, Y (. ] ii ~omment Arrl\le,\ on ~~~~ ,.J rslS p "-r5<!. be~M "-f \":'-,Jt y D lXI D D 0 ~ Pv..r~e ef1dc~ ttl)~ ~IYJ~~~ N specified below) y N y D 3x40m1 D D HCL D D 100 ml D ~ H2S04 B 0 250ml D 0 HN03 0 0 250ml 0 0 No Preserv. D 0 1,000 ml D 0 HNO:l D 0 Sample volume 0 &:1 0 IfpreseiVntive is used, specify Type and Quantity of Preservative: Sample Time See instruction ·~n(ler ~"'\ t'v.r~a w~ll eolledd J G-"'rr•" ?re.~.urr tbr pw~e ()..(\~ SD.fY1pl·'':5 even+: tor 0.... ·h,·hl cr ~ M;llvJe:::... t.Ja.f~r ~CL!. ck-<-ir l'~ZS LeO sr:.k a.+ )'327 N 0 0 D D D 12.1 L-...---""'"'-"'""""'-"-""""'---__;,_Jino not touch this cell (SheetN~e) White Mesa Mill Field Data Worksheet for Groundwater A 2 of2 capturx-COMPATIBLE WrTtl;/"-u.&ti>--rullCfiOHALJU Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I ,~ Q\AM+~· rJi'fr~te zolS See instruction Location (well name): .._l..:-r....:.w..:N..:..-.....::.07..=-----------J Sampler Name and initials: 1...,-;.r'll?e;r H61),J~~/-r).f Field Sample ID Date and Time for Purging I 7.../lg/-aolS and Sampling (if different) .N'/A Well Purging Equip Used: I][) pump or [QJ bailer Well Pump (if other than Bennet) I Gon+inv.ov. ~ Purging Method Used: [QJ2 casings [QJ3 casings Sampling Event I o~('+erl;? /'l ::ho-.+c Prev. Well Sampled in Sampling Event .... l_tV._'/_1\ ________ ___, pH Buffer 7.0 Specific Conductance ._I _I_Oo_o ____ __.l~-tMHOS/ em Depth to Water Before Purging l 33.6b Weather Cond. Time I o~rz.'t I Gal. Purged l ~ Conductance l -z_qL)~ I pH I {;.S~ Temp. oc I 14,...,, I Redox Potential Eh (m V) I ~H I Turbidity (NTU) I 0 I Time I I Gal. Purged I Conductance I I pH I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater I I I I pH Buffer 4.0 Well Depth(O.Olft): I 'l(;,,Dt> Casing Volume (V) 4" Well:l 40,"1~ 1(.653h) 3" Well~~--__ o __ -l.(.367h) Ext'l Amb. Temp. ·c (prior sampling eventl._IZ_0 __ ____. Time I I Gal. Purged I I Conductance I I pHI I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) L I Time I I Gal. Purged I I Conductance I I pHI I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) I I 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flow Rate Q), in gpm. S/60 = I l~.t> Time to evacuate two ca ing volumes (2V) T = 2V/Q =I g:s-z. I Number of casing volumes evacuated (if other than two) D If well evacuated to dryness, number of gallons evacuated 0 Name of Certified Analytical Laboratory if Other Than Energy Labs ._I .:..A:...;Wc....:.;;A..::L:.-_____ __, Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients ~ 0 100 ml 0 ~ H2S04 ~ 0 Heavy Metals 0 0 250m] 0 0 HN03 0 0 All Other Non Radiologies 0 0 250m] 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) IJ'j 0 Sample volume 0 ~ 0 ~ c~lor;Je. If preservative is used, specify Type and Quantity of Preservative: Final Depth ._I_S_7_._1J ___ _, Sample Time o&z.S See instruction Comment Arr;\lecl Ofl ~··t~ a-.+ 0~7:2.. -(Annd" lkf'l~ (j-lil.(f';n p<c:Set\1--1-b Gollec..+ i..~1'11ple~. ~"-fYlp )c~ Go ll c:oc.+~~ o-,.} C ~'Z..S wo-..+er wc..s G )-Gor Left" ~ITe o..+ O<f>7.7 TWN-02 02-18-2015 lDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I I sr Gl v..tt..rtGr A) IJr,..te 2.0 L5 Location (well name): 1~...-r..!....:.w:::.;t\J~-*..::0=~~--------____. Field Sample ID Sampler N arne and initials: See instruction Date and Time for Purging l~.-.:-z::.:./-'l.::..g;'---z._o.;...LS~-----' and Sampling (if different) ._I .;;;Z"""/-'J..;.;q)'--z._o....;.l.;;:;5 _____ ____, Well Purging Equip Used: IT[] pump or @]bailer Well Pump (if other than Bennet) I Gru..1lilfcn Purging Method Used: 002 casings @]3 casings Sampling Event I Gv.o.rterlj 1J;0}1"~tc::. Prev. Well Sampled in Sampling Event ~...l_-r_w_W_-_1 8' _____ ___, pH Buffer 7.0 Specific Conductance l.._lo_o_o ____ _,l~-tMHOS/ em Depth to Water Before Purging I 3 g. q 0 Weather Cond. Time I J9zq I Gal. Purged I Y7.6D Conductance l 73oD I pH I G»sg Temp. oc 1 \s.rs I Redox Potential Eh (m V) I Zl':S I Turbidity (NTU) I -z..O I Time I 0 7 '1'1 I Gal. Purged I 0 Conductance I '2-'2.~ Y I pH I G;.E;o Temp. oc I \':S.Z\9 I Redox Potential Eh (m V) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater I I I I pH Buffer 4.0 L\.0 Well Depth(O.Olft): ._I _,_q_6_.o_o __ ____. Casing Volume (V) 4" Well:,37. Z8 ,(.653h) 3" Well:~... __ o __ __,_(.367h) Ext'l Amb. Temp. ·c (prior sampling eventl~-,;.17_0_6 __ _, Time I I Gal. Purged I I Conductance I I pH I I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Time 1 o'q" I Gal. Purged l o I Conductance I 'l:'Z<'j~ I pH I b5'1 I Temp. oc I r3..2H I Redox Potential Eh (m V) I I Turbidity (NTU) I I 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q) in gpm. S/60 = I 1LD Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two ca ing volumes (2V) T=2V/Q= J b .77 I l l.27 I t.\7.bo Name of Certified Analytical Laboratory if Other Than Energy Labs wl A..._W--'-"[1..._1-_____ --1 Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D D 3x40 ml D D HCL D D Nutrients ~ D 100 ml D !] H2S04 El D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologies D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) ~ D Sample volume D El 0 ~ C.nlona(.. If preservative is used, specify Type and Quantity of Preservative: Final Depth ~..-I _1...;_~,;_.1_) __ --J Sample Time 07Y5 See instruction Comment Arri..>~a 0(1 s.;+~ o.i-I~ 23 ~nne/' tMlJ.. G-Olr(;f) yc~s..eflf J.or ru.r~e. Pv.r~~ .b'G"'11 o.+ 71(<.5 P tA.r~ed well Fof fA. ~o-1-e>~J 0 .f 'i M1nl),.·h~~ D,,ll(l -zo .seconb. f'w-~~J Well .Jrj! PV\.r~c e(l~ea o..+ lY21, LGJ-f ~)tc eo..-d-IL\31. 1.0o...+er ~ I'J'>"~.J-,!j cJ<:~r. An--i\1~6 on s.lfe-o.,} 07YO ~fl~r" MA Gp..rr:n pr~etrf ~ collec-J--s~ples, De.p+h· ..fo ~ ())~ 3S. C:.o f.o..Mp1e.> b~-J~ d o7LfS LeJ} s_;+~ ad-o7Y7 TWN-03 02-18-2015 ]Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER See instruction D~ri~oo~s~~i~E~m: ~~-~~-~_Q_._~_~_~_c_r_~-~-~-~_t_~_z_o_~~----------------~ Sampler N arne and initials: 1-,-;..Ml« Holi:J.r.a.~/11:} Location (well name): 1.__--rw __ N_-_o_q.;...._ ________ __. Field Sample ID Date and Time for Purging I '2./18/2015 and Sampling (if different) I N/~ Well Purging Equip Used: rn::]pump or IQJ bailer Well Pump (if other than Bennet) Purging Method Used: 002 casings IQJ3 casings Sampling Event I Q\Ab..rterb 1\5;-J<~J< Prev. Well Sampled in Sampling Event ._I ~_l_W_JJ_-_0_7 _____ __. pH Buffer 7.0 /,0 pH Buffer 4.0 4.0 Specific Conductance ~~ _l_oo_o ____ _.l ~MHOS/ em Well Depth(O.Olft): I )"2.S., 7/J Depth to Water Before Purging I !;:3,00 4" Well:l 47, g7 1(.653h) 3" Well: o (.367h) '---"'------' Casing Volume (V) Weather Cond. Ext'l Amb. Temp. oc (prior sampling event)._l'?_0 __ _. Time I )"2.53 I Gal. Purged I gg I Time I l&S"i I Gal. Purged 111 I Conductance I \Ot.?:> I pH I c..sz I Conductance I I~ I pHI Gsz I Temp. °C 1 ~05 I Temp. oc 114.72. I Redox Potential Eh (mV) I -z.."ZJ,.. I Redox Potential Eh (m V) I 22!:> I Turbidity (NTU) I 0 I Turbidity (NTU) 16 I Time I 1<.5$ I Gal. Purged I 1)D I Time I IZSL I Gal. Purged I 1Z1 I Conductance I ,0'=3 I pH IG .&-z I Conductance IIOb3 I pH I b.52 I Temp. °C I 1'1.7!:;, I Temp. oc 11q,7z I Redox Potential Eh (m V) I rz."Z.q I Redox Potential Eh (m V) I z:zq I Turbidity (NTU) I C> I Turbidity (NTU) l l> I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged lzJ gallon(s) Pumping Rate Calculation Flow Rate CQ), in gpm. S/60 = I 11. v Time to evacuate two c.:a in volumes (2V) T = 2V /Q = I g' b3 I Number of casing volumes evacuated (if other than two) l o If well evacuated to dryness, number of gallons evacuated lo Name of Certified Analytical Laboratory if Other Than Energy Labs ILA:...;..:.W....:.Pr.;....L.:....._ _____ -..~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y VOCs D D 3x40 ml D D HCL D Nutrients Kl D 100ml D £] H2S04 ~ Heavy Metals D D 250 ml D D HN03 D All Other Non Radiologies D D 250 ml D D No Preserv. D Gross Alpha D D 1,000 ml D D HN03 D Other (specify) ~ D Sample volume D ~ D C~)or·,Jc. If preservative is used, specify Type and Quantity of Preservative: Final Depth IL......=5::....L\,...S.t..:~.__ _ ____. Sample Time See instruction Comment Arr'IIJd; on .si-te o..t )7. 'i l --r;.nnt.(" ll\)1a &o.rr: (l p('~.s..enr +0 ..-ru..r~.e. ~nJ .s ompli:j ¢Ven-t. f v.r~ b~~"n q..t' \-z.qs. 'Pv..r~.d we\\ ~,.-o... ¢-~a..\ of 1\ m:nu.-Tt:s., w4r ~~ c.le(4.r- f1Ar~e, eY1Jea C\na .Y."1p1~~ colled-cl ~-t rz.5(.,.. L-e..f.t sJe ~-s )7..51 TWN-04 02-18-2015 loo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D IB 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I I !.I Qv.M+er A) ,'4fr ~ fc:: "2 o l5 • See instruction Location (well name): ._I _-r_w......;....}.)_-_0;:_7-'---------------' Sampler Name and initials: I ~nn-c.r Hon;J/)~frH Field Sample ID Date and Time for Purging I "2.../ 18/ "ZOJ.S and Sampling (if different) ._I -'~;,;,/...;,11f=J_z_a_;;J.S==--_____ _. Well Purging Equip Used: (![]pump or [QJ bailer Well Pump (if other than Bennet) Gfw''Jfo~ Purging Method Used: 11[]2 casings [QJ3 casings Sampling Event I Qv.o-rftr}Oj .N •'::J:o..f~ Prev. Well Sampled in Sampling Event I l vJAJ-0 7 R. pH Buffer 7.0 -,, "D Specific Conductance!._ _\_O_D'O ____ _.I ~-tMHOS/ em Depth to Water Before Purging I 8' S. tf 0 Weather Cond. Time I .Jz-z.\ I Gal. Purged I 16.50 Conductance I )253 I pH 17./l Temp. oc I \ 4.7'1 I Redox Potential Eh (m V) I -z.5z I Turbidity (NTU) I 0 I Time l673j I Gal. Purged lo Conductance I l·z:z.~ I pH I (; .. '2..0 Temp. oc 1 r3,,4g. I Redox Potential Eh (m V) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater I I I I pH Buffer 4.0 Y.D Well Depth(O.Olft): )05,0l> Casing Volume (V) 4" w ll:,Jz,4] ,(.653h) 3" W~II:.__O;;,.,..._ __ _..C.367h) Ext'l Amb. Temp. oc (prior sampling eventliLS=-"----' Time I I Gal. Purged I I Conductance I I pHI I Temp. oc I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Time I073b I Gal. Purged IO I Conductance I rz..::si I pH I t;.=zs I Temp. oc 119.61 I Redox Potential Eh (mV) I I Turbidity (NTU) I I 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged lb. SO gallon(s) Pumping Rate Calculation Flow Rate (Q) in gpm. S/60 = I II. D Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casjn T = 2V/Q = z:z4. '--------J \.3Z. Name of Certified Analytical Laboratory if Other Than Energy Labs I.__A"""'W___._A.;._t.. _____ ___. Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D D 3x40 ml D D HCL D D Nutrients ~ D 100 ml D [29 H2S04 ~ D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiol{)gics D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) ~ D Sample volume D IE D ~ G 'hJ M~ Je If preservative is used, specify Type and Quantity of Preservative: Final Depth ,_I ..;_10_3 ..;.... '2..5=-__ _. Sample Time I D73S See instruction Comment Arr;\)~~ on ~;+~ ,.-r 1217. ~Mo-e(' lhtl~ G-M-r;n pre.se"1-..f;(' }> ...... r~e. 'Pv..c~-e b~.311'-fl e-.t IZGO ~v..r6e~ 'ilcll .for ~ tohJ of \ Mt'ntA.tG 30 .S~c.ofl!.S. PIA,r~d. well .jr.j~ VJ"'t~ w~ cJe.a.f'. fv..r~-e cndd. o.t 1-z"ZJ. L.,.i)-si·J-c ~ 1-z.z~ Arri\.le~ Ot\ sii-e. ~-t 0731 lMner" ~ 6-AS"r'•n 'f'r'GS.e.I\J-+o eollc:ct SOJo<Jplei. D~r-th -Jo wo.fer waS qs.g~ ~o.)Y\pks ~;le.A cr---Y 07~S LeJi. ~i't-e. a..t 0737 TWN-07 02-18-2015 loo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I I ~T Q~o>.o.rter 1\);j.-r.-.otoe: 20 l5 See instruction Location (well name): ~.--1 _l""[W_N_-_0_7__;_R;;..._ _______ __J Sampler N arne and initials: 17"41\ntl~t"" Holl;~~/'1f;l Field Sample ID Date and Time for Purging l._ __ '2...__,_/.:....:l~"--'/_2_0_1....;;5;;..._ __ _. and Sampling (if different) Well Purging Equip Used: ~pump or @]bailer Well Pump (if other than Bennet) Purging Method Used: @]2 casings @]3 casings Sampling Event I CJAo-<toc:rb N ~•he~~c Prev. Well Sampled in Sampling Event ~.-I_P_i~_'Z_-_0_1 _____ __, pH Buffer 7.0 /,0 Specific Conductance ._1_'0_0_0 ____ _.1~-tMHOS/ em Depth to Water Before Purging ~.-1---'o:;__ __ __. Weather Cond. Time I llSb I Gal. Purged I \'"Z..l Conductance I z.o I pH I g. '3.5 Temp. ac 111105 I Redox Potential Eh (m V) I Z:Zl:3 I Turbidity (NTU) I 0 I Time I I Gal. Purged I Conductance I I pH I Temp. ac I I Redox Potential Eh (m V) I I Turbidity (NTU) [ I White Mesa Mill Field Data Worksheet for Groundwater I I I I pH Buffer 4.0 4.0 Well Depth(O.Olft): ,__o ____ _. Casing Volume (V) 4" Well:~...,.o----il(.653h) 3" Well:. 0 . (.367h) Ext' IAmb. Temp. oc (prior sampling event)..._[ =g -o __ _. Time I I Gal. Purged I I Conductance I I pHI I Temp. ac I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Time I I Gal. Purged I I Conductance I I pHI I Temp. ac I I Redox Potential Eh (m V) I I Turbidity (NTU) I I 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q , in gpm. S/60 = I 'l. 0 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T=2V/Q= I 0 t lo Name of Certified Analytical Laboratory if Other Than Energy Labs ._I _A_W_ft_L _____ ___.l Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D D 3x40 ml D D HCL D D Nutrients l!J D 100 ml D EJ H2S04 n D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologies D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) r!J 0 Sample volume 0 "t:l 0 ~ c n \o(J'dc. If preservative is used, specify Type and Quantity of Preservative: Final Depth L-1 _o ____ _. Sample Time See instruction Comment Art'i~d 0(\ ~~.}~ ,d-\ 1'-\b IMn~ Ar~P.. G-o.rr:n pr~el1t .for r•Yl.SO..i-e. 'R;,~+c=.. b~11 Af HYS 'P\A.Mf'~ 5.0 Cr#-llot1~ of' Sl'>~ L&A.i-~r-Ml~ lol> G-,.n ~r.s 6f ~I w"+~r . 'R ;()_s"' ·tc: ~nJeJ. a-..t 12oo .YAM f l eS CO II ec. 1-~ J o. t 11.57 Lett SJ'-1-c (}J \'Z.DZ TWN-07R 02-18-2015 lDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill -Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I l ~-r ai.).D..r+cr j\) ;=!""('o...f~ "Z.O I5 Location (well name): ~...1 -r....:....;;.W.;;.<tJ.__-...:....1 %=----------' Field Sample ID Sampler Name and initials: See instruction Date and Time for Purging I -z./11!./zors I and Sampling (if different) I IV/.4-7.../)VZOJ5 '---....:....:...:: _______ --.~ Well Purging Equip Used: OOpump or [QJ bailer Well Pump (if other than Bennet) 1~..-:&...;..r_l-\:...nd;;..;.~..;...C\S....;;.._ ___ --.~ Purging Method Used: 002 casings [QJ3 casings Sampling Event I Q~r+e.rb f\)1-}.fAf< Prev. Well Sampled in Sampling Event l._-ri_w_JJ_-_0_1 _____ _.. pH Buffer 7.0 (,0 pH Buffer 4.0 4,0 Specific Conductance ~...1 ...;..lo_o_o ____ _.h.tMHOS/ em Well Depth(O.Olft): I IY5,Db Depth to Water Before Purging I 59,7g Casing Volume (V) 4" Well:l $.by 1(.653h) 3" Well: 0 (.367h) '--------' Weather Cond. Ext'l Am b. Temp. ·c (prior sampling event).._l ..._'l_0 __ _. Time I 1%~ I Gal. Purged I ~j I Time I 1~5~ I Gal. Purged I )JO I Conductance 1 -z.:vn I pH I C:. .l" I Conductance I 22.~2. I pHI b,IZ:O I Temp. oc I 1"1.53 I Temp. oc I \4 .53 I Redox Potential Eh (m V) l bt;j I Redox Potential Eh (m V) I l"iCJ I Turbidity (NTU) I 0 I Turbidity (NTU) I 0 I Time I 'goo I Gal. Purged I ]-z. 1 I Time I 19 01 I Gal. Purged ll3"Z I Conductance I 7..7.~0 I pH I c;.n: I Conductance I -z.'L'"i1 I pH I G;.lb I Temp. oc I 1q .159 I Temp. oc I \9.!)6 I Redox Potential Eh (m V) I ,7~ I Redox Potential Eh (mV) I 178' I Turbidity (NTU) I 5 I Turbidity (NTU) I 0 I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate Q , in gpm. S/60 = l IJ.D Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V/Q = l IO .• l 1 I 0 Name of Certified Analytical Laboratory if Other Than Energy Labs A\-JAL Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D D 3x40 ml D D HCL D D Nutrients 1!1 D 100 ml D 1!1 H2S04 l!l D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologies D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) [] D Sample volume 0 ~ 0 ~ c~'or:J~ If preservative is used, specify Type and Quantity of Preservative: Final Depth ._I ...::;b:....:..l.;.:;.,£?~---.J Sample Time See instruction Comment .Ar6 \1~~ Of\ ~it-t; ~l l3Y5 -r;.,ne,... D./I). GArr;" pfe.Sc:,.,-1-' .£(' pur~~ ~na .SAJY~_p);~ .. ~hJe"'} Pv..r~e be~MI ~+ 13"1~ 'Pv..r ~f~ w~JI .fc,,.. tl\. i-o+AI of IZ t'Vl;,L\1-0 . w.Jd' W4.S cl~r p w~~ -enJGA GS\r'l~ Sa1Y1p\e5 collect~~ ~t )YDJ. Left S,Tc ~} )~05 TWN-18 02-18-2015 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I \ 5-T Gh'-D-r+e,... Gh loro'f'orm "o IS ~ See instruction Location (well name): l.._-r_\J_4_-_z_z _________ __. Sampler Name and initials: l...,.-oo./\11 ef"" HoJJ ,'J'!!1hJ1 Field Sample ID Date and Time for Purging J 3/4 / Z.O lS and Sampling (if different) I N/.4 Well Purging Equip Used: [Q)pump or [QJ bailer Well Pump (if other than Bennet) Purging Method Used: [QJ2 casings (g]3 casings Sampling Event I my-\i Ch )o.roForrY) Prev. Well Sampled in Sampling Event I "TWLJ-Zlf ~---------~ pH Buffer 7.0 7.0 pH Buffer 4.0 L.\.0 Specific Conductance ._l_10_o_o ____ _.l!!MHOS/ em Well Depth(O.Olft): l._11_3_.s_o __ _J Depth to Water Before Purging I sCi. b 7 Casing Volume (V) 4" Well:! ~5. \S ,(.653h) 3" Well: o (.367h) L--------' Weather Con d. Ext'l Amb. Temp. oc (prior sampling event)IL._IO_" __ ~ Time I I:>~ I Gal. Purged I 0 I Time I I Gal. Purged I I Conductance I l;Oi.3 I pH I l;:zg I Conductance I I pHI I Temp. oc I 15 , .. l,.;> I Temp. oc I I Redox Potential Eh (m V) I zz:;o I Redox Potential Eh (m V) I I Turbidity (NTU) I D I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (mV) I I Redox Potential Eh (m V) .1 I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flow Rate (Q , in yrn. s16o = 1 n. Time to evacuate two ca. in g volumes (2V) T=2V/Q= I :b.qy I Number of casing volumes evacuated (if other than two) 0 If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs AWAL Sample Taken Sample Vol (indicate Filtered Type of Sample if other than as y N specified below) y VOCs "tl D 3x40 ml D Nutrients rn D lOOm! D Heavy Metals D D 250 ml D All Other Non Radiologies D D 250 ml D Gross Alpha D D 1,000 ml D Other (specify) 'ttl D Sample volume D Ch 1oriJe. Final Depth 1~..-V_._-z.:_:z. ___ ..~ Sample Time Comment A(r~V!e.'a on s.~te 01.t 1333 ~M~' s~tvlple..s. LO llec.f~A "'-t 13.3(, M} (r,.,,.;., pres.efl+ +o ~a.·h~r I.U~ G l-eof leQ ~;-k ~~ 133~ c~ Y\"flnLAOIA...) ?v.rYlpi~ Well TW4-22 03..09-2015 I Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N ~ tl D D D tl Preservative Type Preservative Added y N HCL ~ D H2S04 f!j D HN03 D D No Preserv. D D HN03 D D D r!J If preservative is used, specify Type and Quantity of Preservative: See instruction 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (OAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL see instruction FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I I~ T G V..l).r:l¥ ch lor aFore'\ z o lS Sampler N arne Location (well name): I -Jw'1-2j and initials: I ~fln~r Ho li,·Ja!1/nt Field Sample ID Date and Time for Purging I 3/q / -uJJS and Sampling (if different) L-1 .:...rJ....!/~A...;._ _______ ..J Well Purging Equip Used: (IDpump or [QJ bailer Well Pump (if other than Bennet) I C.o11 "fi t'h.A.OV.~ Purging Method Used: fiD2 casings @]3 casings Sampling Event Qv..o-r-+~rl.;\ Ch\orotorm Prev. Well Sampled in Sampling Event ._l--n_w_Y_-_45 ______ _, pH Buffer 7.0 7. () pH Buffer 4.0 4.0 Specific Conductance L-l_lo..;..o..;..o ___ ---lh.tMHOS/ em Well Depth(O.Olft): ._I _I l_Z_.S_o __ ____...J Depth to Water Before Purging I b q · g D Casing Volume (V) 4" Well:' 3-l.l~ ,(.653h) 3" Well:L-. ....;;.o ___ _._(.367h) Weather Cond. Ext'l Amb. Temp. oc (prior sampling event)l._1_o_o __ __, Time 113-z..£, I Gal. Purged I 6 I Time I I Gal. Purged I I Conductance I :z 59~ I pH I 6.ZY I Conductance I I pH I I Temp. oc I 1 5.1.1 I Temp. oc I I Redox Potential Eh (m V) I "'22.Q I Redox Potential Eh (m V) I I Turbidity (NTU) I D I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. °C I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate Q), in ~m. Time to evacuate two ca ing volumes (2V) S/60 = I 17 . T=2V/Q= I 3 .iK I Number of casing volumes evacuated (if other than two) 0 If well evacuated to dryness, number of gallons evacuated 0 N arne of Certified Analytical Laboratory if Other Than Energy Labs I.__......;A....;....;.vJ_A"'" ..... 1 _____ __, Sample Taken Sample Vol (indicate Filtered Type of Sample if other than as y N specified below) y VOCs _r:;;l D 3x40 ml D Nutrients ~ D 100 ml D Heavy Metals D D 250 ml D AIJ Other Non Radiologies D D 250 ml D Gross Alplw D D 1,000 ml D Other (specify) l5ll D Sample volume 0 L'h1or;~(. Final Depth I 73.97 Sample Time Comment White Mesa Mill 01"1 ~.-+<. a-.1-1~"2.'3 collec.hj ~>..r I3Z~ 11.t l~Z~ -r;.i\(\C,(' ()..(\ ~ G-o.. r r; t1 ?'~'"-LS.ert+ IN&.. ·h,... wo0 G I ea. r TW4-24 03-09-2015 IDo not touch this cell (SheetName) Field Data Worksheet for Groundwater N Qf og D D D rB Preservative Type Preservative Added y N HCL ~ D H2S04 ~ 0 HN03 D 0 No Preserv. D 0 HN03 D 0 0 lj If preservative is used, specify Type and Quantity of Preservative: See instruction 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER DescriptionofSamplingEvent: I 1~1 Qv.o..,.{er G"'lor<)Fortv"' ZOI5 See instruction Location (well name): l.._~-·~w:::.L1_,_·-__;;;?.5:=.. ________ -J Sampler Name and initials: I ~llfler Ho JI;JQ;\ /7ft Field Sample ID Date and Time for Purging I 3/'1/v>.J.S and Sampling (if different) ...VIA Well Purging Equip Used: ~pump or [ill bailer Well Pump (if other than Bennet) Purging Method Used: 1][12 casings 1][13 casings Sampling Event I Qv..~rtc.rl; Cb lorofor,.., Prev. Well Sampled in Sampling Event .._1_-rT_W_Y_-_Jq _____ __, pH Buffer 7.0 /,Q pH Buffer 4.0 Y.o Specific Conductance l.___lo_o_o ___ ___.l!-l-MHOS/ em Well Depth(O.Olft): Depth to Water Before Purging I :S 7. ~ D Casing Volume (V) 4" Well:,SO.LJ I ,(.653h) 3" Well: 0 (.367h) .__..;;;._ __ _, Weather Cond. Ext' IAmb. Temp. ·c (prior sampling event).._l1_0 __ ---.~ Time I )"2.5 'I I Gal. Purged I 0 I Time I I Gal. Purged I I Conductance I 'Z.~GJl I pH I b.5C.. I Conductance I I pHI I Temp. oc I )S.OO I Temp. oc I I Redox Potential Eh (m V) I P·'9 I Redox Potential Eh (mV) I I Turbidity (NTU) I 0 I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flow Rate {Q), in gb. S/60 = I ) b .o Time to evacuate two casing volumes (2V) T = 2V /Q = I b 3D I Number of casing volumes evacuated (if other than two) 0 If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs I,_..:.A.:..\J......:..:.A-=L'-------" Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y VOCs 151 0 3x40 ml 0 ~ HCL 5I' Nutrients [1:1 0 100 ml 0 rgj H2S04 rn Heavy Metals 0 0 250m! 0 0 HN03 0 All Other Non Radiologies 0 0 250m! 0 0 No Preserv. 0 Gross Alpha D D 1,000 ml D 0 HN03 0 Other (specify) I:B D Sample volume 0 00 D Ch lol"ide If preservative is used, specify Type and Quantity of Preservative: Final Depth I 7 y. ~y Sample Time See instruction Comment A<ri\Je~ 0(\ si+e oo..i-)Z57 ~01'Vlple.s. c.ollec+ed o...t l...e4 ~1te. ~+ 130~ ..,-;_fl'fle.r o.11l G-o.rn'rr presell.f +o co/lec..f-:S,t~mfles, 1300 VJ~ter w~ c.lea.r C a Yl f-~ Y7 u o v._s TW4-25 03-09-2015 lno not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 li 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER See instruction ~~~ooclS~~~~m: ~l~\S_T_Q~·~-~_r_+~~-r-~C~k_l_o_r~d g~o~r-~--~-o_l_5 _______________ ~ Location (well name):j .._ _""'f'-W"--L\,_--=6=-b __________ _. Sampler Name and initials: J ::r;:-,..n-e.r H6JI,·J~-::ifrH Field Sample ID Date and Time for Purging l.__3.:;::;.:..../.:...:17c.<./....::;'Zo....O..:..IS..~-------' Well Purging Equip Used: O[)pump or ~bailer Purging Method Used: ~2 casings ~3 casings and Sampling (if different) .__AJ....;/,_~=----------l Well Pump (if other than Bennet) I 6-rv.Mlfos, Sampling Event I Q'""o..r fer{.j .CJ\ lorol"~('m Prev. Well Sampled in Sampling Event l .... _M_W_-_3_~ ______ _, pH Buffer 7.0 7,0 Specific Conductance ._l __ lo_o_o ___ _,I!!MHOS/ em Depth to Water Before Purging I -::z:t;:t-6--D I Weather Cond. Time I OK ~!J I Gal. Purged l 0 Conductance I "!;,~ I pH I 7.12 Temp. oc I '1~,9:3 I Redox Potential Eh (m V) I ~!50 I Turbidity (NTU) I Z.l I Time I I Gal. Purged I Conductance I I pH I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater I I I I pH Buffer 4.0 y.o Well Depth(O.Olft): 0 Casing Volume (V) 4" Well :11--:0,...----11 (. 653h) 3"Well:_ () _(.367h) Ext'l Amb. Temp. oc (prior sampling event)J.__'2_o_· _ ___. Time I I Gal. Purged I I Conductance I I pHI I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Time I I Gal. Purged I I Conductance I I pHI I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) I I 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flow Rate (Qt in gpm. S/60 = I 0 Time to evacuate two casing volumes (2V) T = 2V/Q =I 0 I Number of casing volumes evacuated (if other than two) 0 If well evacuated to dryness, number of gallons evacuated 0 Name of Certified Analytical Laboratory if Other Than Energy Labs ... I_A_\J----'A..:...L.:._ ____ _j Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs n D 3x40ml D tJ HCL ~ D Nutrients rJ D lOOm! D a H2S04 Ll D Heavy Metals D D 250m] D D HN03 D D All Other Non Radiologies D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) ~ D Sample volume D 1!!1 0 ~ Gh1o.-:k If preservative is used, specify Type and Quantity of Preservative: Final Depth .._l __ o ___ --J Sample Time I ()g5S See instruction Comment TW4-60 03-17-2015 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill-Groundw.ater Qischar&e Permit ( ( O;~te: 06-06-12 Rev. 7 2-Errata Ground~'ilter Monbring Quality Assurance Plan (QAP) ATIACHMENT 1-2 WHITE MESA URANIUM .1\flLL FIELD DATA WORKSHEET FOR GROUNDWA 'FER Description of Sampling Event: 1 ~1 QWI..Jer N ~·±r,•.1e 20/S Location (well name): ._I =-f.......:w;.;../J_-_,£:;..;;0 _________ ___. Sampler Name and initials: Field Sample ID '-l 11.:..:w:..;;lw~\....:_G==~::..:::-~c-=z-~..J9J..:z::..:o...:...,l.f.~....· _____ _.l-rw....,-r;.u _ cz1q z..ol5 Date and Time for Purging I Z./lj holS and Sampling (if different) Well Purging Equip Used: OOpump or [QJ bailer Well Pump (if other than Bennet) Purging Method Used: @]2 casings @]3 casings I G I ~ I -rwN-o3 Sampling Event G "'o.c[Gd!:\ t.Ji.l·'} tc; Prev. Well Sampled in Sampling Event ._ _________ _. pH Buffer 7.0 7.0 pH Buffer 4.0 '4,0 Specific Conductance ._l_~o_o.;...o ___ __.J!J.MHOS/ em Well Depth(O.Olft): I 0 ..._ ____ __. Depth to Water Before Purgingl ,_ _t. __ ~ casing Volume (V) 4" Well:r_o ___ -t,(.653h) 3"Well:_ o _(.367h) Weather Cond. C lc=(;.r Ext' I Am b. Temp. •c (prior sampling event}._l 2~0::..." __ _. Time I 0709 I Gal. Purged I 0 I Time I I Gal. Purged I I Conductance I \.L I pH 17.31 I Conductance I I pHI I Temp. "'C 1)2 -2 '1 I Temp. oc I I Redox Potential Eh (ruV) I \(~q I Redox Potential Eb (mV) I I Turbidity (NTU) I li'L I Turbidity (NTU) I J Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I J Temp. °C I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I -I Turbidity (NTIJ) I I White Mesa Mill Field Data Worksheet for Groundwater A 1 of2 Capturx· tOM.ATIO~[ WITH/'-UU'lir--FUNtTIDNALIT¥ Mill-Groundw<~ter Discharge Permit Ground.X.;rter Monhori1111 Qu•~tv AssUr.nce Plan (QAPJ ( ( Date; 06-06-12 Rev. 7.2-Err.ta Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60= I 0 Time to evacuate two casing volumes (2V) T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) l o If well evacuated to dryness, nwnber of gallons evacuated l o Name of Certified Analytical Labornto:ry if Other Than Energy Labs ._.I A .... W~A'-=L-'---------' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs 0 0 3x40 ml D D HCL D D Nutrients ijJ 0 lOOmi D ~ H2S04 ~ 0 Heavy Metals 0 D 250m! D D HN03 0 D All Other Non Radiologies 0 0 250ml 0 0 No Preserv_ 0 0' Gross Alpha 0 0 1,000 mJ 0 0 HN03 0 0 Other (specify) 6:1 0 Sample volume 0 I&J 0 I§ _c h\-o n1 If preservative io; UBed, specifY Type and Quantity ofPreservative: . lFinal Depth I C i ~--~-----~ Sample Time ! E :\Comment · 4 See insrruction f.:-r .. DI )~ C\+ 07i0 ~----------------~ Do not touch this cell (SheetName) White Mesa Mill Fit!ld Oat.. Worksheet for Groundwater A 2 of2 capturx-COMPATIBlE WITH.,..-'L.....,zi:r--FUHCTIONALITV Min, Groundwjlter Discharge Permit ( Date: Of>.06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) I ! l " ;; ? i?l)--..-~ "~~~~!MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description ofSamplingEvent: I j!fl"" &Mde/" G'fo~.f'd..'4{hi ZOL5 Sampler Name Location (well name): 1-rw/J • b~ and initials: Field Sample ID Sec insbUctJon Date and Time for Purging I -z./J~/'Z.¢15 and Sampling (if different) #/A ~----------------~ Well Purging Equip Used: ~pump or [gJ bailer Well Pwnp (if other than Bennet) 6-ri.An(\f.;~ Purging Method Used: @2 casings @]3 casings Sampling Event I ~l)..r-\-erlj 6-\t) .AJ ,1 r.,_"fc: Prev. Well Sampled in Sampling Event l.__-r_I.J._tJ_-_0_~-------' pH Buffer 7.0 pH Buffer 4.0 I 4.o Specific Conductance ._I _lO_D_o ______ ___.lllMHOS/ em Well Depth(O.Olft): I i IZ .5D Depth to Water Before Purging I bD, 8$ Casing Volwne (V) 4" We.ll:l '33./0 ,(.653h) 3" Well:_ o (.367h) ._ ___ _. Wenthcr Cond. Ext'l Amb. Temp. •c (prior sampling event)l~-:'f~"-------~ Time I I Gal. Purged I I Time I I GaL Purged I I ' Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. °C I I Redox Potential Eh(mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) L I 'Fime I I Gal. Purgecl I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. °C I I Temp. oc I I RedoxPotentiaJ Eh (mV) I I ' Redox Potential Eh (m V) I I Turbidity (NTIJ) I I Turbidity (NTIJ) I I White Mesa Mill Field Data Worksheet for Groundwater .A 1 af2 capturx· CQM~ATIDL• WITH/'-,_n,--FUHCTIONALITY Mill c Groundwater Discharge Permit Gruundw;~ter Monitoring Quality Assurance Plan (QAPJ ( Date. 06-06-12 Rev. 7.2 -Errata Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Ql~ in I:,'Pm. S/60 = I ., j,O Time to evacuate two casing volumes (2V) T=2VIQ= I b 12 I Number of casing volumes evacuated (if olher than two) I D Ifwell evacuated to dryness, number of gallons evacuated I o Name of Certified Analytical Laboratory if Other Titan Energy Labs 1'--'-"AlO""Jf""'L _____ _. Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other lhan as Preservative Type y N specified below) y N y N VOCs D D '3x40ml 0 D HCL D 0 NutrienfS ~ 0 '100 ml 0 ril H2S04 B 0 H~''Y Metals D 0 QSOml 0 D HN03 0 0 All Other Non Radiologies 0 I< 0 250m! 0 0 No Preserv. 0 0 Gross Alpna 0 0 l.OOOml D 0 HN03 0 0 Other (specify) Iii D Sample volume 0 fi.:l 0 .s C 'hlor;Je If preservative is usl:d, specifY Type and Quantity of Preservative: Sample Time I:?.J25 ~omment (J See instruction . : .__ _______ _.!Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Grour1dwater A 2 of2 capturx· COMPATIIL£ WITH.,/'-<"'o.nr-FUNCTIONALITY TabC Kriged Current Quarter Groundwater Contour Map, Capture Zone Map, Capture Zone Details Map, and Weekly, Monthly and Quarterly Depth to Water Data NAME: Garrin Palmer, Tanner Holliday DATE: 3/26/15 Depth to Depth to Depth to Depth to TIME WELL Water (ft.) TIME WELL Water (ft.) TIME WELL Water (ft.) TIME WELL Water (ft.) 1300 MW-1 64.10 1212 MW-4 71.20 1245 PIEZ-1 64.52 NA DR-I ABANDON 1327 MW-2 109.74 1213 TW4-J 72.08 1238 PIEZ-2 37.09 NA DR-2 ABANDON 958 MW-3 82.71 1211 TW4-2 74.79 1235 PIEZ-3 47.98 937 DR-5 83.25 958 MW-3A 84.81 1218 TW4-3 55.50 1243 PIEZ-4 56.30 934 DR-6 94.28 1319 MW-5 106.35 1214 TW4-4 72.00 1240 PIEZ-5 55.57 1307 DR-7 92.31 1248 MW-11 86.43 1220 TW4-5 63.33 1217 TWN-1 61.00 929 DR-8 51.22 1321 MW-12 108.47 1235 TW4-6 70.75 1214 TWN-2 29.98 926 DR-9 86.71 1254 MW-14 103.38 1212 TW4-7 72.50 1227 TWN-3 38.30 924 DR-10 78.26 1257 MW-15 106.35 1216 TW4-8 74.51 1232 TWN-4 52.70 952 DR-ll 98.40 1004 MW-17 72.34 1221 TW4-9 61.24 TWN-5 ABANDON 955 DR-12 90.66 1257 MW-18 71.59 1223 TW4-IO 61.12 1254 TWN-6 77.65 1001 DR-13 69.96 1241 MW-19 60.47 1210 TW4-ll 91.00 1303 TWN-7 85.93 920 DR-14 76.50 852 MW-20 85.72 1024 TW4-12 44.95 TWN-8 ABANDON 947 DR-15 93.11 847 MW-22 66.90 1023 TW4-13 50.44 TWN-9 ABANDON DR-16 ABANDON 1313 MW-23 114.40 1019 TW4-14 81.91 TWN-10 ABANDON 916 DR-17 65.02 1314 MW-24 113.44 1209 TW4-15 67.90 TWN-11 ABANDON DR-18 ABANDON 1243 MW-25 75.73 1225 TW4-16 65.00 TWN-12 ABANDON 905 DR-19 63.20 1209 MW-26 67.90 1228 TW4-17 77.00 TWN-13 ABANDON 903 DR-20 55.52 1310 MW-27 53.78 1221 TW4-18 64.10 1248 TWN-14 61.56 856 DR-21 101.35 1318 MW-28 75.46 1045 TW4-19 63.40 TWN-15 ABANDON 913 DR-22 DRY 1324 MW-29 101.10 1206 TW4-20 63.88 1250 TWN-16 47.66 859 DR-23 70.72 1321 MW-30 75.49 1223 TW4-21 61.16 TWN-17 ABANDON 909 DR-24 44.36 1229 MW-31 68.26 1202 TW4-22 72.00 1230 TWN-18 59.79 NA DR-25 ABANDON 1228 MW-32 77.00 1230 TW4-23 67.90 1034 TWN-19 53.40 1303 MW-33 DRY 1200 TW4-24 65.88 1302 MW-34 107.96 1225 TW4-25 57.51 1312 MW-35 112.50 1237 TW4-26 65.25 1310 MW-36 110.64 1010 TW4-27 80.23 1259 MW-37 107.49 1025 TW4-28 38.89 1018 TW4-29 73.00 fOB TW4-3U 76.58 IDI1 IW4-31 lli.Z:i 1027 TW4-32 50.49 1008 TW4-33 71.59 1016 TW4-34 70.97 1014 TW4-35 74.31 1021 TW4-36 56.80 1204 TW4-37 60.17 @ estimated dry area TW4-37 temporary perched monitoring well +5572 installed March, 2015 showing elevation in feet amsl MW-5 perched monitoring well showing e 5503 elevation in feet amsl TW4-12 temporary perched monitoring well 0 5579 showing elevation in feet amsl TWN-7 temporary perched nitrate monitoring Q 5563 well showing elevation in feet amsl PIEZ-1 perched piezometer showing loil 5591 elevation in feet amsl TW4-35 temporary perched monitoring well ~5526 installed May, 2014 showing elevation in feet amsl RUIN SPRING 6 5380 seep or spring showing elevation in feet amsl HYDRO GEO CHEM,INC. H:/718000/may15/WUUwl0315 _rev.srf FIGURE C-1 , ,, .. estimated nitrate capture ,' 1' zone boundary stream tubes I resulting from pumping estimated chloroform capture zone boundary stream tubes resulting from pumping @ estimated dry area TW4-37 temporary perched monitoring well __.,._5572 install~d ~arch, 2015 showing ...,.... elevat1on 1n feet amsl MW-5 perched monitoring well showing e 5503 elevation in feet amsl TW4·12 temporary perched monitoring well 0 5579 showing elevation in feet amsl TWN-7 temporary perched nitrate monitoring ~5563 well showing elevation in feet amsl PIEZ-1 perched piezometer showing Q 5591 elevation in feet amsl TW4-35 temporary perched monitoring well ~5526 installed May, 2014 showing elevation in feet amsl RUIN SPRING b 5380 seep or spring showing elevation in feet amsl HYDRO GEO CHEM,INC. KRIGED 1st QUARTER, 2015 WATER LEVELS AND ESTIMATED CAPTURE ZONES WHITE MESA SITE H :/718000/may15/ nitrate/Uwi0315NTcz2_rev .srf ,' , TV!:I,:1-37 T ssn MW-4 .5551 TW4-7 0 5549 PIEZ-2 "'5592 TW4-35 ~5526 estimated nitrate capture zone boundary stream tubes resulting from pumping estimated chloroform capture zone boundary stream tubes resulting from pumping temporary perched monitoring well installed March, 201 5 showing elevation in feet amsl perched monitoring well showing elevation in feet amsl temporary perched monitoring well showing elevation in feet amsl perched piezometer showing elevation in feet amsl temporary perched monitoring well installed May, 2014 showing elevation in feet amsl NOTE: MW-4, MW-26, TW4-1, TW4-2, TW4-4, TW4-11, TW4-19, and TW4-20 are chloroform pumping wells; TW4-22, TW4-24, TW4-25, and TWN-2 are nitrate pumping wells HYDRO GEO CHEM,INC. KRIGED 1st QUARTER, 2015 WATER LEVELS AND ESTIMATED CAPTURE ZONES WHITE MESA SITE (detail map) APPROVED DATE H:/718000/ 15/nitrate/Uwi0315NTcz_rev.sri FIGURE C-3 Weekly Inspection Form ( System Operational (If no note T' arne W II e D h* ept c om ments anyero bl t ems corrective actions} -MW-4 -Flow -Yes @ Meter -Yes(f\fOj -MW-26 -Flow --Yes (N3) Met,er ---Yes ~ j.300 TW4-19 67.42 Flow I \.o &P.M. yeS) No Meter 3onE\I uo ~No -TW4-20 ---Flow --Yes (N ~ Meter -Yes (Nq --TW4-4 -Flow -Yes QJO) -Meter -Yes ~ ,.._ 1414 TWN-2 'J,Z.6.o Flow l~ Z /sP,AA. ~ No Meter 37 S'l LIT .So (Le) No TW4-22 -Flow -Yes (NO) Meter -Yes (Nq -TW4-24 ---Flow --Yes (NO) Meter ----Yes (N{_)) ~ 14\D TW4-25 62.00 Flow 16. ~ &f'_AA. eYe~ No Meter I o 10 ct 9 4 .10 (YeS\ No - Operational Problems (Please list well number): Ml..J-4, M 0-U, ·n.v:\-zo1 1"W:\-lj . =rw<-\-Z.~, r;.v'-1-'Z.l{ A o+-aeCrJ;A.t•el\o.. (, Qi~£.\..v.r(,~ \.~., EN~Je,...A.. t\)e-,y \. ..... <. S ~u !cA. be,_ Corrective Action(s) Taken (Please list well number): --------------- " Depth is measured to the nearest 0.01 feet. I \ Weekly Inspection Form Date Time Well DePth* Commei1ts \.~Cf MW-4 7D s£ Flow 4.g 6-PJA 1s~ MW -26 -"1_2 • '13 Flow 12. o t.-f #'\ Met,er Litg0.530-41 1404 TW4-19 ..S'LI'-t Flow 152g TW4-20 b'1 53 Flow g _{) &P~ Meter 46025 L.f5 Meter Z7'1ltl-l 6o tsu: TWN-2 4l.30 Flow 1 fS.Ll &PM Meter 37ff61r\ 1m 1s2.5 TW4-22 £o. 2l Flow n. 4 &r'.M 15 2z TW4-24 _65.'63 Flow Ji .. ~ ~"""' Meter 110 '-~37_1 Cjl) 1s;'"{ TW4-25 51r.7 ~ Flow IA.'"lk-~M Meter rot~-JID 'to Svstem Operational (If no note anv problems/corrective actio ns) (Ye§\ No f{es No t(e§) No Yes@ Yes (No) {Ye$ No {Ye~ No rfe]) No Ke§> No d9ID No (fe~ No -~No eve&::> No CiW No (Ye~ No <fe$) No Operational Problems (Please list well number): :CI.s?'-1-ltt soa.s + (.clpare.r, !'{ sk • .!/i 4££ alv~ :+o fcobls.""""s t+? i tl-""'CM:~ cJ-,Sc.~£.-\ •.-.e.. Corrective Action(s) Taken (Please list well number): . No j., £;cJ.. M&..iv. +v-~u. to r-e.pc.. .c \ i""-C • r Depth is measured to the nearest 0.01 feet. Weekly Inspection Form ( System Operational (If no note Tl me Wll e D th* 9D1 c t ommen s an)l ero bl I . I ) ems corrective act ons ~~ L.lb MW-4 70.'11 Flow y_.s (,P.J-'\. O'eS, No Meter :Sbl~2'1 . 3:3. 6'eS) No 143~ MW-26 /..~.60 Flow \Z..Q &()~ t(e~ No Meter 1.1 ra.7/1 ,3o /?e~ No - 11..\0) TW4-19 66_.Q_6_ Flow 1-z.o GPA (Yes) No Meter '30il75 7 6. 00 n':e~ No 1 '-t'3o TW4-20 66.62.. Flow ><.t.. 6.P~ .tfes No Meter 473£8'.03 <fe~ No 1453 TW4-4 10.\0 Flow i I. ~ t;.PA (Ye~J No Meter 36ii.GO ~\.No lU.Lo TWN-2 "32.6.\ Flow 17.0 &P.M. (Y'eS')No Meter 3922..62' I-\ 0 e_re5)No 14Z7 TW4-22 61.\.ctr Flow 1SL D GP,..v\. (yes) No ( Meter I q:3 Cot lf'1.30 <Ye~ No -=- llo\2"1 TW4-24 6-il.'iS" Flow n.q M~ (Je_S)_ No Meter n 1.s,;s 1. 1o (Yes.) No 1~13 TW4-25 ..ss.os Flow I L\. 5 &P"'"' (feS., No Meter 101~'16.60 (Y'"e0 No ~.50 TW4-1 b'LD5 Flow I g. 0 G-f....v\.. ~No Meter Z.oil .oo (Y'e$) No I 441 TW4-2 (O.t) Flow 1~LO 6-PA (Yes) No Meter Z.&.IS-7. I 0 ~No 14.3S TW4-11 6'i.20 Flow 1~to yPM. tf_e§) No Meter l4b7. co ~S> No ' -TW4-21 Flow Nc.-t ;A-' Yes l:NJ)) -O{Je..r-&>.. ~ 0-""- Meter -Yes )<fo) - Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): ---------------- * Depth is measured to the nearest 0.01 feet. ( Weekly Inspection Form ( Date 1 f.2.12lts Name System Operational (If no note Time Well Degth* Comments anv nroblems/corrective actions) _l~.5J MW-4 72. 45' Flow 45 &-PM (Yes) No Meter ..£f.g'7~1.()~ 7Ve5) No \441 MW-26 h~-6i Flow I z.o &PM... ((§.~ No Meter 4~.!:"4.o.lf~ (YeS No ~ 141L\ TW4-19 63 gg Flow IZ .0 6-P..M.. ~es) No Meter 3103t)7 \ ./")(":) (?eS) No J 1.{3_g TW4-20 6'5.6Y Flow ~-4 &P.M (Yes) No Meter 4g6~4 .10 ffe§) No 1457 TW4-4 70.04. Flow \\.D 1$-P..AA-tY-es) No Meter ifi .. '1!07. ry.) (VeJ) No 14'2'3 TWN-2 3V~5 Flow l S. '2. &fAA.. rf':ej> No Meter .3~11611 .1..\,Q ~No I LI3L\ TW4-22 _6_3. I L{ Flow J~.o f.., PM ~s/No ( Meter l 'I 5"3~5 .(D 2(e_s} No 14.31 TW4-24 /,£. 2._~ Flow 17.g &P.I"''-. (Ye$' No Meter 17 ·2.62 2.3. YC> ~No 14.24 TW4-25 90 . i'-\ Flow 1'7,:3 (,-\>.~"\. (fe5) No Meter I0'12Z.\7. 36 /\'e!?') No -_..,. I '{S!.f TW4-1 /()_.00 Flow J((D &RM cf__e§.) No Meter 454Z-.6o (Ye~_)No \'-1.1.\~ TW4-2 /Z,\D Flow l lis'. D C ... P .J-".. &es )No Meter ""' ~ . -s2s-c_q-e ({es) No 1~.41.{ TW4-11 13.51 Flow ,g.o &(-l,.v\.. t!{ej) No Meter :S4!i'S. 10 (Y'ej) No !:::>- ~ TW4-21 --Flow N ~ + '""' ~o~r-... +; t. ....... Yes {No) Meter -Yes (1\JO) - Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): ---------------- * Depth is measured to the nearest 0.01 feet. Monthly Depth Check Form Date "r..~( IS" Name W..r'"'""" Pc..l-u-{ T:Mfr tklLky Time Well Depth* Time Well Depth* 1 zz.g MW-4 ·Jo.D6. 12.31 TWN-1 6.0--:1. I 1235 TW4-1 1().()5 lZ.l~ TWN-2 ::tz..6 B IZ,'Z..~ TW4-2 ::z:z.4b \ 'Z.~O TWN-3 3'\.0Q !:Z:~l TW4-3 5$.11 lZ.'-{3 TWN-4 5 :1. ~7 Jz.;p TW4-4 J.O. 9g \'Z.S'I TWN-7 ~.'1.5 )'2.16 TW4-5 63-ZS ll!:i~ TWN-18 5~.68 1:?.40 TW4-6 70.~0 I:Z..!::U MW-27 SJ..I D IZ.L.~ TW4-7 6 :r .l~ l:?:.S6 MW-30 !S.4( 11:3Z. TW4-8 I l.gQ I~S MW-31 &~-~7 l:Z19 TW4-9 61.17 IZ.IS TW4-10 61.()~ I 'Z. "2.( TW4-11 1l,8.D t:'cj TW4-12 L~~.Ll\ I:>D'i:. TW4-13 Ll't ,c;g I 3.1 ( TW4-28 ~g.£~ 136~ TW4-14 ~z ~1 ~ 1Ja3 TW4-29 :J~-18 I'Z.Q9 TW4-15 (27 .\"Z. 1:200 TW4-30 J.6~J 1303 TW4-16 65'-&: I l'ZS~ TW4-31 ~1.3> ll.Sb TW4-17 11..1.\Q 1~1~ TW4-32 .5Q.1\ l~3j TW4-18 ~:\-D!l IZ.4g TW4-33 ]\.,30 IJ.J3 TW4-19 6_5.1 L. 12..5'1 TW4-34 1(2.6,g '~!27 TW4-20 6.5.8?... )3o2-TW4-35 1LI. 25 I~ TW4-21 6 'Z -~6 l::;c,b TW4-36 .S6,li~ I'Z.o~ TW4-22 ~(!). t:t] 124'-TW4-23 67-55 1'20~ TW4-24 bl..o?... I Db TW4-25 .5'1.00 II.Y:( TW4-26 6t.l.qQ l'Z.S5 TW4-27 ~o.'Z-~ Comments: (Please note the well number for any comments) * Depth is measured to the nearest 0.01 feet / ' ( Date -z-/z./ zo '!:> Time Well Depth* \-.,1[) MW-4 7'1 . .35 J':)30 MW-26 bg_'ib ·cYflS TW4-19 6760 l3~ TW4-20 7(.. '-l~ tSDi TW4-4 b:,9,93' ~ TWN-2 iS:10 13S7 ~3,0 I~Oq TW4-22 7'1.'-.\L. 1 ~0(, TW4-24 k.b. \2.. J35 t TW4-25 60.lG\ I-t r-i.+ TW4-1 7"' 4K 1::)1~ TW4-2 '7S.IO l3 z..5 TW4-11 qY.qK #/A TW4-21 /V/4 Weekly Inspection Form Name ~r'}cr fb J!tJ1) Comments Svstem Operational (If no note anv problems/corrective actions) Flow Y.F. G-.PN'\ _{_ Ye~ No Meter S7.5LJ Zl.\ .97 ~No -:::;:.._ Flow t·-z..D _(Yes)No Meter '-\~~qK.q7 ?'Y'e~No -""' Flow 1-z.. C) (Yes) No Meter 3J 097:) '2... o 8' ~No ........ ../ Flow x. l {rf!-'\ (-v_~s) No Meter 4 qg ~.b ~No Flow 10.1 G-t'M _('lis No Meter 1570'; h ( Ves ) No - Flow ..,., ~m lZS.Y ~ (Yes) No ' Meter -ra ;:· 3~'r~{::.1 N _eYe~ No -;>=< Flow n.qo _{'(es..2No Meter !'172 IC.... b (YeS) No --Flow 1~-0 lY_e~ No Meter \'13(.,)1.19 (Ye~No Flow 16.1 (YeS) No Meter l 072. '-\1. g (Y9) No ~ Flow 17.5 (Ye~No Meter 702.5.7 (Yes)No - Flow 1/.3 G-PM ~No Meter 19 SL{.~ (YJ¥g No Flow ~~~.o frP.M ('Yes)No Meter 5 I Ob :1 (~No Flow -~~4 Yes(' No ) Meter IV'/A Ye&'"N~ Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): --------------- *Depth is measured to the nearest 0.01 feet. ( ( Weekly Inspection Form Time Well Depth* Comments 1 J.'Z7 MW-4 81.2o Flow _'-i . .s' 6-f'#\.. Meter .rgz:z~'-t;,o 1~-1.>q MW-26 Flow 1 tJ , 5 &P ).A._ I '-\oS TW4-19 Flow ll () t-rP.#\- Meter ·w37_3 1 . 06 1'-IS.S TW4-20 6S'.oo Flow g, '6 f-..PA Meter 517.csz. 3D IJ.33 TW4-4 70 7~ Meter z. \ • '2... v ._~o 144.5' TWN-2 Flow 1 S?. ~ t:rrM.. l4.5'l... TW4-22 ;;o ~ <15 Flow 11 ~ %' t,.PA. ,, IL\4~ TW4-24 65 .i Flow ~ Cd/"\... Meter 1"1YS'-t6'!..1o IL\1-{l TW4-25 .5 ~L l? I Flow I 6. c & I' ,.A.. Meter , o•-z.·z..-z.il . 6o t33o TW4-1 Meter 4 '-137 YJ t3'2.'-t TW4-2 13.t.lf) Flow · 1 .1'? &PA Meter i oS~&. RO J32.o TW 4-11 q 1. -z.o Flow 1 g .o t;-V.M.. Meter £g/ q, 7D TW4-21 Flow Meter Operational Problems (Please list well number): Svstem ODe rational (If no note any problems~orrectlve actions) 6'eSJ No ~No ("{e~No ~No (YeS-._ No ~ No /Y9§) No lf_es) No (Yej) No (Ye~ No (YeS) No (Yes) No (Y_e.Y No (Ye$> No (Yw No (Yes) No (Ye~ No ~No ((~No _(YeS) No Cf9SJ No {(8l) No Yes No Yes No Corrective Action(s) Taken (Please list well number): ---------------- * Depth is measured to the nearest 0.01 feet. ( I \ Weekly Inspection Form Time Well Deeth*' Comments \L{(JD MW-4 I '1 '-Ill Flow 4.4 &fM Meter .<: E f< f<,(() ~I i~w MW-26 6E-3\ Flow 17..0 &iM Meter 4lil.s4l1 .o~ I z.'-lb TW4-19 61..507 Flow \\.0 [ANI.. Meter 31 \oo~l. t'J 1 IJII TW4-20 ,t; •-L Z "1 Flow 8.1 &P.M. Meter 52S47 vo I 34'-{ TW4-4 ID.'-1\ Flow II-"Z. (d/A Meter "':"155.J.. "J3 \30F> TWN-2 T:S.o£ Flow jf:,Lj &PA Meter 396~0'2. I :11 '-1 TW4-22 ~q .qo Flow IS'.U (,.{' _,v\. Meter 2.oo '1~3' .StJ I~~\ TW4-24 6.5.3..~ Flow 17 • .8 f:r.f'A Meter I 7 530t,i. ~D \~-1~'"\ TW4-25 ..Sis.ol Flow \5.o b-PJV"-- Meter l~lZ."Z ?,7 . oo t3Y(.J TW4-1 '"1 \.50 Flow IB.D (~~_,.v.... Meter \\.5<;> \(I \~Z£ TW4-2 71.'-IO Flow Meter t""Z.ll ~ 7. 70 13'23 TW4-11 ll 'i. 70 Flow l gcO &f.' A Meter tss6. 10 'n,a~ ~\Aj ~ / -Mete"'t---' Operational Problems (Please list well number): -LcJJI fote>c..r-b1 Tk>'-1 -~ • 4 Svstem Ooerational llf no note a~obleins/correctlve actlonsj d~.§)No c..Ye~ No fl_es2No ('Y'e$) No .=- (fes )No 7feS1) No ----(Yes~ No (VeS, No /Y..el No rve~No .... _(Y~ No (Y'e~ No _Lf~ No ~No ~e§l No «._~No (Y_eS) No LYIDNO _(YN_) No _(Y~No Yes cf@ Yes ®.a> /"'fe~ No ("f'e§\ No VA~ ..r-Jo ~Ne- Corrective Action(s) Taken (Please list well number): £I ec.. +r 'lt:.t (j!A s L-..611 <--bee-A A ' 1-: C: e.. cA. ~""""' " * Depth is measured to the nearest 0.01 feet. Weekly Inspection Form Date :z.l-z. r..l( 1 4 System Operational (If no note Time Well Deeth"" Comments anv Problems/corrective actions\ li '\o 6 MW-4 ~O.t.')O Flow 4.6 &Pfo"' {Y'e~ No Meter 5%4 &''l • TZ. (yej No ogs\ MW-26 65.70 Flow I Us G-PJ"\ (Ye:) No Meter 4'1314 93 58 ~No ...... 0~0,:!.4 TW4-19 f.J3.6o Flow ~ _ 2 &P /A.. {'i'es) No Meter 312.3~15.00 ~. No n~4f. TW4-20 64.60 Flow ~.o GP.A <Ye~ No Meter 54 lo g '2.3 f(eS) No oct18 TW4-4 IC1.4"Z.. Flow 1c>.o &P.AA... )(8S) No Meter 4131.-{o\S 40 ?re'ID No osz.g-TWN-2 33.2~ Flow 18.8 Gf'~ ~No Meter '1. 60 6._5' \{. 7 0 ('i'e_s) No ~~'-{0 TW4-22 A.Z . 4 o Flow \1. t;, G.-P~ KeS\ No Meter 'ZO 3D ~.L '(0 ~)NO OS3'-I TW4-24 bS.zo Flow .I ~L.t"~ &r"""-tYe~..)N.o Meter II{, 30 "l 7 Jie::, ~s-'\No C>K2.3 TW4-25 57.~" Flow f.._ c._ (:C~-V\. c'Y'Ets) No Meter IDrZZ..5CS.'iO eYes\ No - 6GI12. TW4-1 '11.30 Flow lf_g kf'M-~No Meter \4116., '-1.0 ~No --0'101 TW4-2 (4 .$10 Flow 1-, 3 r~rAA ('(es_."No Meter i5'374.5D (Yes)No CfiJS'] TW4-11 qz.so Flow \'l!.Q f-P~ ~No Meter 11-50.0\ d:e]) No TW4-?1 --.... ~-law-...., Yes~ Meter --.....__ Yes c:"lSl.a> Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): • Depth is measured to the nearest 0.01 feet. Monthly Depth Check Fof~ Date z_{zL.t/1&.\ Name R c..rri ..-P"'-\t<:"\:§C Time Well Depth* Time Well Depth* oq~6 MW-4 So.oo IQO!:j TWN-1 60.7'-t D'HZ.. TW4-1 ]1.30 D~z..~ TWN-2 33.ZZ. Q90I TW4-2 ::z~. iJQ I O:f-6 TWN-3 3S. 25 1:3~3 TW4-3 .S!:!.~b 1.:31'-TWN-4 52.65 C2qll TW4-4 IQ.l-{2.. TWN-7 S7.SS I:!>Zj TW4-5 63-0D TWN-18 fi&"t3 5~.66 D~V TW4-6 7o.3S lOI6 MW-27 5:3.56 1.:13~ TW4-7 ll. 65. 1'·-\ :?,~ MW-30 :::z~. 3$5 1335 TW4-8 7~.3D 1 'i3b MW-31 tS.'36 IJ>I TW4-9 60 .~L.J I~LL TW4-10 6.'b . fiZ. 6~51 TW4-11 gz.so ~41'"2... TW4-12 4~. 'ZS I :IIC2 TW4-13 ~9 . .St I "il~ TW4-28 .3S'. 56 I~D6 TW4-14 S 1. 'l o I ~o4 TW4-29 1"2.~61 ( 0~5:1 TW4-15 65;70 12t5'5 TW4-30 J6.~30 I 1~1~2 TW4-16 .6S.t6 TW4-31 gi.C>7 1~1 I~Jo TW4-17 7,.60 l~lb TW4-32 l)o.09 100/ TW4-18 6_3.q3 l~!::l9 TW4-33 11. z.s 6~~~ TW4-19 ·6'l.60 }4.00 TW4-34 (0 • .56 Q:<ll'!:i6 TW4-20 6~-bD 1:357 TW4-35 ]4.09 lt21Q TW4-21 61.75 ~~~i TW4-36 56.-6a o~~a TW4-22 &:2...40 13LIZ-TW4-23 67.~ ~ :i ~~~!::l TW4-24 f.5~U> 6i'23 TW4-25 57-fb 13'-~Y TW4-26 64-8j 1351 TW4-27 So. e:>Z Comments: (Please note the well number for any comments) * Depth is measured to the nearest 0.01 feet Weekly Inspection Form Date 3 / 'Z-1 1!\ Time Well Deoth* Comments 151'\ MW-4 Flow 4..6 M'M Meter &:::>2.'-\. 2..'2..oo LSD~ MW-26 ~~t.:YZ.. Flow u .. o &Ptv\. Meter 4 u.s o <L 't i J 416 TW 4-19 61..~"18 Flow s.o &~.}A Meter >rz..11.{ l5_oo t5o4 TW4-20 £4. .. :.>'-1 Flow q,o &PM Meter !')54 g 7. 7 l 1528 TW4-4 7o. LO Flow ID .O M.-A Meter ~'liOO. 'lo tLns TWN-2 )\.'15 Flow ts,'{ ~,..A Meter Lio31ll&. "o 1 <{.5'& TW 4-22 Meter ZD4.76?.6o l<.t50 TW4-24 Flow 1 1. '-l t.-().M Meter t76'lZ.S6 .6o IY'2..7 TW4-25 57.37 Flow 16.0 lrt'~ Meter lG>72.362. 80 1523 TW4-1 Flow 1 fl .o 6-{l.IA. Meter tblt5'.4D Lt;t14 TW4-2 /4.50 Flow 11. 4. c's-f...v\. Meter 111 f(/, so 151\ TW4-11 Flow 1 K.o 61>.#'- Meter 7781.'1D TJAI.ct--£ I Flow --- Operational Problems (Please list well number): ILc.elG:.C.-e..ol l....c.Ai '"""'f Is I<JL.f.-'2. Corrective Action(s) Taken (Please list well number): * Depth is measured to the nearest 0.01 feet. System Operational (If no note any problems/corrective actions} ~No l(e$) No (Ye~ No /("e~ No -..., ~No rYe~ No /rei> No eYes) No C!~ No (Ye_s) No (VeS)No (Yes.) No 6'~ No (Ye_i) No ~No (Yes)No (Yes') No ~ No (Ye_s) No Yes No res No Weekly Inspection Form Time Well Deoth* Comments 14Js-MW-4 71:. ,Qo Flow t.t.b &r~ Meter 6oct"l-:z.Ct . 92... 1357 MW-26 70 .D6 Flow \""Z. ... o &?~ 12.00 TW4-19 L311:2 TW4-20 Meter 5 6 g-q_s-. o '{ tt.go TW4-4 7o.oo Flow 1 t.o t:Fry.._ Meter '-1'-li'}/ s<o l.51i TWN-2 Meter 4oT'. 17. 6o 133'-TW4-22 sq,67 Flow n.g-&P~ Meter 2o~$J'4 .3D 13Z.'-{ TW4-24 /:Joo TW4-25 57.bD Flow 16.o Gf~ tY4Z.. TW4-1 Sl.oG Flow Meter J4Z7 TW4-2 75 2o Flow 1 'if. o ~__.<A._ Meter 1 oo 61 lo 14os TW4-11 Meter snz. '-1o T~ ____.., Meter "-.. Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): ... Depth is measured to the nearest 0.01 feet. System Operational llf no note any problems/corrective act1ons) /'7es )No {Y"es) No &S)No ~ No (Ye?;J No l(e8; No (Yes No ('r"e~ No f("es)No Cf~No (Yes) No ?YeS) No CYes')No (Yes""'\No (Ve~ No ~No (YeS) No ;Ves) No ~No (YeS) No (fiS) No ?'(ej.)No /'_Yes} No -Yes No ~es~ Weekly Inspection Form ( Svstem Oceratlonal (If no note Time Well Oe_Dth* Comments any problems/corrective actionsJ l "3-~ i MW-4 7 ~-f/6 Flow LL 7 r..-P;V~... (Y'es) No Meter 6' 100,.:; Q' T2.. ~No ~ f<.S7 MW-26 /c_q &-Flow II 5 6,-(J_..v\. (Yes) No Meter t..lt.fq.5g'; Zo ~No ~ \C...( I.{ <is' TW4-19 hZ.61i Flow i 'Z..o &P..v\.. ( Ye.s) No Meter .3136r.SS'.oc> ("{ej) No --... n:.tq TW4-20 ~3. S'f Flow q~z. f-.R _,.(./~, .. ((~No Meter .15 ~ z..~ 3 . '-(o (Lei) No ~~~ TW4-4 7o.oo Flow t I.~ ~.;V\_ /Ye_s} No Meter !;O~~ISLr' ?re~ No ..::::::::-... fT1,~ TWN-2 z.q..oo Flow i~Ls· &-P.M.. Ct&VNo Meter '-1110 L{£,70 (Ye$) No l3'-l~ TW4-22 scr. '1 Flow J~.o &P.....-\. ;Y~No Meter '2.~ !lL\C\o. t'o (Y~ No ~ 134 2.. TW4-24 7q,o3 Flow i '5 6 M...u\... Cfej) No Meter 17 ~I f.Z.,~. 3o ('rej)No 133.5" TW4-25 _57,5€ Flow 16.0 &f'A ;f~)No Meter 1072.306. '-iO (Ye_s~ No -::::::.-.. 1'-105 TW4-1 /'l... ~0 Flow 17 h ~P.M.. ~No Meter Z.0\15 .W t!l_e.$' No ~ \.35-b TW4-2 7£.6ct Flow i 7 ~ U.P!-A-(Yej) No Meter ?o7~o.72.. !Y'E!s) No 13...1~ TW4-11 'i 0. g_s-Flow 11?. 0 &P_,....._ {'(es ..-No Meter ~810_ Z/') lfe~ No i.J:lA.-"+-£ I -t-Flow Yes .ble--- ~ -•v•.::aer -~---_.....yes No Operational Problems {Please list well number): Corrective Action(s) Taken (Please list well number): ---------------- • Depth is measured to the nearest O.Q1 feet. Weekly Inspection Form Date 3/z.s/,s Name 0a..r-c;<> Pcz (~ /1 ~ t{oLL~J."'f System Operational (If no note Time w ell eot c omments I . ) an:l£ Qroblems corrective actions 1 ... , '2. "' MW-4 lb,otl Flow 1-\.6 &~.-"-'\. (Yes >Jo Meter ~ZYL{b'Z. Z-5 (Ye_s) No 1 ~u ct MW-26 67.50 Flow 'l-b C,{J_,AA-Lie~ No Meter Sc>Z .. 5"'t.l OR" CYe~ No Ji-1515 TW4-19 ~6>.9'i Flow \?'.6 frP/o-A.. (fe~ No Meter 3142S~Tec em No ~ ,._.,6. TW4-20 /,J ,50 Flow 'Lz lH'..AA-. (Yei No Meter t-,o IDi 17 ?feS') No II.{J_I} TW4-4 7c>. '-/ z... Flow I \.t> &P-M ;re5J No Meter 57556-50 (re__s) No 140/ TWN-2 Z-~.41 Flow j&.O f-r-f/J'-(Yes) No Meter 'ii571L5b rrel No :-.... I 1..l1 Y. TW4-22 7l.(')5 Flow 17. ~ &V'.M.. ('Y'eyNo Meter 2l D t;<?..,'Z. So ("(eS) No - 11-\IG TW4-24 t.:'Lt 4'5 Flow n. s> r$'" _,.\A ('re§) No Meter 11~1654 .. '\R 6eib No \'-lO 3 TW4-25 t;) '-15 Flow lb .. D C,.f')A.. (Ve§> No Meter lO~Z31"1.40 ('Yej) No 14Y2... TW4-1 7Z_ C..f'J Flow 11.4 &P..M.. Yt6S) No Meter 2.26()'3. 40 aeg No '- 142& TW4-2 IS 3.1 Flow \l.L.{ &P_.A.-\ {Yes)No Meter zz.q A'· -z.s-~ No l'-tz.3 TW4-11 t:to. {,o Flow tf.o (;.p....,.__ fis) No Meter '1t....J6L\ ll Cf_e~ No ..--~21 ~ I~ ----1--:::---... Yes No / ...___ v----Mete~ ...._~~ Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): * Depth is measured to the nearest 0.01 feet. Weekly Inspection Form System Operational (If no note Time Well Deoth* Comments anv problems/corrective actions} _1_113'1 MW-4 7 3 .2.\ Flow 1.4 .I. 6-p """-~No Meter -'"Z.'l o3/,, R, ~No ,., \4~0 MW-26 /Z.•-H Flow ll 2. &-P.M. t!l~) No Meter 5b3.,.q5.5o ~No <".. l_S_I!)" TW4-19 k'1 . 4 (jc Flow Jl .o G-PA. (Y~ No Meter -:\14./S~ 1.5.ou (tej) No .-.. lL.t27 TW4-20 ~~L3o Flow q_~ G-P.M. ({~ ~)No Meter i. w-t n ~ tJ6 lfe U No .:::::.. 1141.(5 TW4-4 IZ..•·H Flow 11.0 '"""""' ~ P No Meter 61~"-"0 ('(ej ~ No __:-,. I 1.\17 TWN-2 Z.i'. "}7 Flow li." bP.-IA <Ytas\No Meter 1.118::312. &.lO (Ye~ No ....,_ ILi"Z.t-\ TW4-22 61.1."it Flow 11.1!: M~ <Y.as) No Meter Z I Z.OI 6 • .:3D (Ye~ No " 11.{2.\ TW4-24 b4. 7A Flow _n.'3 (rf,w\ CYe~ No Meter lllii'Z.l.ct.U::. 8e$) No \&.tit.\. TW4-25 SI.'-LS Flow I ~ .o t~P~v.. (Yes) No Meter IOIZY.~~-1.0 (Ye~ No .... I "4 4 '2. TW4-1 TZ. :z.:z. Flow \1 ,t &P..M. CYe.._cU No Meter Z4S6'1. Zo &es~No _.........._ \1.\3/. TW4-2 {{,,'-t"l. Flow 1'7' '\ UP/A ("l'~ No Meter "2.L\\St.7o (Y..es) No 1'-tS3 TW4-11 'lo::n Flow n .1 (rP-"" ~No Meter .,.S"'IIL -zo (YPSJ No ITWfi-?1 lftow. Yes No Meter "--_.-. ......._ ... ~ NO Operational Problems (Please list well number): Corrective Actlon(s) Taken (Please list well number): ---------------- * Depth is measured to the nearest 0.01 feet. TabD Kriged Previous Quarter Groundwater Contour Map @ estimated dry area MW-5 perched monitoring well showing .5503 elevation in feet amsl TW4-12 temporary perched monitoring well 0 5580 showing elevation in feet amsl TWN-7 temporary perched nitrate monitoring <> 5563 well showing elevation in feet amsl PIEZ-1 perched piezometer showing g 5591 elevation in feet amsl TW4-35 temporary perched monitoring well ~5526 install~ ~ay, 2014 showing elevatron rn feet amsl RUIN SPRING b s380 seep or spring showing elevation in feet amsl HYDRO GEO CHEM,INC. KRIGED 4th QUARTER, 2014 WATER LEVELS WHITE MESA SITE H:/718000/feb15/WUUwl1214.srf TabE Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells -a. E -.c .a:: -Q) E i= a.. ~ 0 Q) > Q) ...J a.. Q) -~ ,.. I z ~ 9~/0~/90 8~/H/80 G~/~0/170 0 ~/8 ~/ ~ ~ 60/90/LO 80/GG/GO - 0 c) 0 c) 0 c) C\1 0 c) v ~ 1 j ~ 0 c) It) ~ ~ ~ I 0 c) CD 0 c) " -c. E -.c = -Cl) E i= :I.. Cl) > 0 Cl) > Cl) ...J :I.. Cl) -ca 3: N I z ~ 9~/0~/90 s ~~v~;so <::~HO/vO 0~/8~H ~ 60/90/LO 80/GG/GO 0 0 0 LC) C! 0 ~ ~ ~~ { ~. 0 Lt) ,.... 0 0 C\J ~ [> r--" ~ ~ ~ / C! 1.{) C\J 0 0 C') C! 1.{) C') 0 0 '<t 0 1.{) '<t ~ 01 0 ~ 0 0 I ~ ~ ~ Depth Below Measuring Point (ft.) w 01 0 w 0 0 I ~ ~ ~ ~ ~ t ~ 1 I I ) ~ ~ 1\) 01 0 1\) 9 0 I ...... 01 0 I ....... 0 0 I 01 0 0 0 02/22/08 07/06/09 ~ 11/18/10 z I (,J ~ -CD ""''i r-CD < ~ 04/01/12 0 < CD ""''i ::f 3 CD -= . C' -08/14/13 3 "C - 12/27/14 05/10/16 -a. E j5 = -(L) E i= :.... (L) > 0 Ci) > (L) ...J :.... (L) -~ llll:t I z 3: t- 9~/0~/SO 8~/17~/90 G ~/W/170 0~/9~H ~ 60/90/LO 90/GG/GO - 0 c) 0 c) ,.... 0 c) C\J 0 c) (') ~ ~ ' ~ 1 \ ~ 0 c) """ ) 0 c) l[) ~ ~ 9 ~/0 ~/90 ...----.------r---,,-----...----r------r----.------, -a. E £~/v~/80 -.c = -Cl) E i= '-Cl) > 0 C:~H0/170 Cl) > Cl) ...J '-Cl) -ca 3: CD I 0~/8~H ~ z ~ 60/90/LO · 80/C:C:/GO -1-----+-----t----+---+----+----t----+-----1 (·u) JU!Od 6upnseaw Motaa 41daa -a. E -.c = -Q) E ;= 11.. Q) > 0 -Q) > Q) ..J 11.. Q) -~ ...... I z ~ 9 ~/0~/SO 8~/17~/80 6~/~0/170 0~/8~H ~ 60/90/LO 80/66/60 - 0 ..¢ CXl ~ 0 <ri CXl '1 ~ "~ ~ > \ ~ 0 <ri 0> 0 cri 0> 9 ~/0~/90 ' -c. E .0 ~ -Q) 8~/v~/BO E i= ... Q) > 0 -~ Q) r--r--~ ~ ~ 1\ ~ '1 ...J ... ~ Q) -C::~/~0/vO ~ ~ ,.. I z \ ~ ~ / ~ .__ r--. 60/90/LO 9~/0 ~/90 ,-----,--------.----.-------,----;--------, -a. E .c ~ --G) 8 ~/17~/80 E i= llo.. G) > 0 a; > G) .J llo.. G) -C:~/~0/170 ca 3: CD ,.... I z ~ 60/90/LO +------+----l-----1-------1-------t-------l -c. E -.c = -C1) E i= ""' C1) > 0 C1) > C1) ..J ""' C1) -~ co ~ I z ~ 9~/0~/SO £~/17~/80 C::~/~0/170 60/90/LO - 0 0 0 0 ..- 0 0 C\1 0 0 C') ~ ~ ~ ~ ~ ~ ~ f::::: ~~ ~ ~ 0 0 ""'" ~ ~ ~· ~ 0 0 1.{) q 0 CD 0 0 1"- -Q. E -.c ~ -CD E i= .._ CD > 0 CD > CD ...J .._ CD -~ en 'r'" I z 3: 1- 9 ~/0 ~/SO -,-----,------,----..-------.----.----.,...-----. 8 ~/17 ~/80 . G~/~0/170 60/90/LO 1-----t----+----+----t----t-----+------t q N lL) ~ N lL) 0 c-j lL) lL) c-j lL) 0 -.:t lL) lL) -.:t lL) 0 ll) lL) ~ lL) lL) -Q. E -.Q . = -C1) E ·-1-... C1) > 0 -C1) > C1) _J ... C1) ... m 3: 0 M I 3: ~ 9 ~/0 ~/SO ,----....,.-----.--------.-----,-----.-----, 8~/P~/80 • c~HOIPO · 0~/8~H ~ 60/90/LO - 80/GG/GO 90/0~/0 ~ S0/8c/SO +-----+-----!-------+------+-----1-------1 0 L(') I' 0 co 1'-- 0 a:i 1'-- 0 0 00 CX> 1\) 0 CX> 9 0 Depth Below Measuring Point (ft.) -...J CX> 0 -...J 0) 0 -...J .j>. 0 -...J 1\) 0 -...J 0 0 0) !X> 0 0) 0) 0 05/28/05 10/10/06 02/22/08 s:: == I (...) ...... 07/06/09 ~ -CD -.: r-CD < CD 11/18/10 - 0 < CD -.: ::t 3 04/01/12 CD -:= C' -3 "'C 08/14/13 - 12/27/14 05/10/16 TabF Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Water Levels and Data over Time White Mesa Mill -Well TWN -1 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,646.96 5,648.09 1.13 112.5 5,600.38 02/06/09 47.71 46.58 5,599.99 07/21109 48.10 46.97 5,600.26 09/21109 47.83 46.70 5,601.10 10/28/09 46.99 45.86 5,602.59 12/14/09 45.50 44.37 5,600.55 03111/10 47.54 46.41 5,600.66 05/11110 47.43 46.30 5,599.18 09/29/10 48.91 47.78 5,598.92 12/21/10 49.17 48.04 5,598.29 02/28/11 49.80 48.67 5,597.80 06/21/11 50.29 49.16 5,597.32 09/20/11 50.77 49.64 5,597.15 12121111 50.94 49.81 5,596.54 03/27/12 51.55 50.42 5,596.52 06/28/12 51.57 50.44 5,595.03 09/27/12 53.06 51.93 5,596.62 12128/12 51.47 50.34 5,593.54 03/28/13 54.55 53.42 5,592.38 06/27/13 55.71 54.58 5,591.65 09/27/13 56.44 55.31 5,590.34 12/20/13 57.75 56.62 5,590.03 03/27/14 58.06 56.93 5,589.09 06/25114 59.00 57.87 5,588.15 09/25/14 59.94 58.81 5,587.74 12/17/14 60.35 59.22 5,587.09 03/26/15 61.00 59.87 Water Levels and Data over Time White Mesa Mill -Well TWN-2 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Elevation Length Of Date Of Water Water Depth Of (WL) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5,626.69 0.94 95 5,611.37 02/06/09 15.32 14.38 5,610.63 07/21/09 16.06 15.12 5,609.73 09/21/09 16.96 16.02 5,607.08 11102/09 19.61 18.67 5,606.57 12/14/09 20.12 19.18 5,612.45 03/11110 14.24 13.30 5,612.78 05/11110 13.91 12.97 5,611.37 09/29/10 15.32 14.38 5,610.24 12/21110 16.45 15.51 5,610.64 02/28/11 16.05 15.11 5,609.78 06/21111 16.91 15.97 5609.79 09/20/11 16.90 15.96 5609.72 12/21111 16.97 16.03 5,605.69 03/27/12 21.00 20.06 5,605.67 06/28/12 21.02 20.08 5,603.03 09/27/12 23.66 22.72 5,605.76 12/28/12 20.93 19.99 5,598.28 03/28/13 28.41 27.47 5,594.32 06/27/13 32.37 31.43 5,594.38 09/27/13 32.31 31.37 5,594.68 12/20113 32.01 31.07 5,597.79 03/27/14 28.90 27.96 5,595.80 06/25/14 30.89 29.95 5,587.67 09/25114 39.02 38.08 5,592.66 12/17114 34.03 33.09 5,596.71 03/26/15 29.98 29.04 Water Levels and Data over Time White Mesa Mill-Well TWN-3 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,633.64 5,634.50 0.86 110 5,603.77 02/06/09 30.73 29.87 5,602.37 07/21/09 32.13 31.27 5,602.34 09/21109 32.16 31.30 5,602.60 10/28/09 31.90 31.04 5,603.12 12/14/09 31.38 30.52 5,602.90 03/11110 31.60 30.74 5,603.23 05111/10 31.27 30.41 5,602.86 09/29110 31.64 30.78 5,603.35 12/21110 31.15 30.29 5,602.89 02/28/11 31.61 30.75 5,602.75 06/21/11 31.75 30.89 5,602.40 09/20/11 32.10 31.24 5,602.40 12/21/11 32.10 31.24 5,601.70 03/27/12 32.80 31.94 5,601.67 06/28112 32.83 31.97 5,600.50 09/27/12 34.00 33.14 5,601.74 12/28112 32.76 31.90 5,598.60 03/28/13 35.90 35.04 5,597.18 06/27/13 37.32 36.46 5,597.36 09/27/13 37.14 36.28 5,597.60 12/20/13 36.90 36.04 5,598.00 03/27114 36.50 35.64 5,596.34 06/25114 38.16 37.30 5,596.30 09/25114 38.20 37.34 5,596.55 12/17114 37.95 37.09 5,596.20 03/26/15 38.30 37.44 Water Levels and Data over Time White Mesa Mill -Well TWN -4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,641.04 5,641.87 0.83 136 5,601.47 02/06/09 40.40 39.57 5,604.26 07/21/09 37 .61 36.78 5,605.02 09/21/09 36.85 36.02 5,605.87 10/28/09 36.00 35.17 5,605.81 12/14/09 36.06 35.23 5,605.31 03/11/10 36.56 35.73 5,605.36 05111110 36.51 35.68 5,604.59 09/29/10 37.28 36.45 5,604.42 12/21110 37.45 36.62 5,603.69 02/28/11 38.18 37.35 5,603.36 06/21111 38.51 37.68 5,602.82 09/20111 39.05 38.22 5,602.79 12/21/11 39.08 38.25 5,600.82 03/27/12 41.05 40.22 5,600.84 06/28/12 41.03 40.20 5,598.47 09/27112 43.40 42.57 5,600.86 12/28/12 41.01 40.18 5,595.57 03/28/13 46.30 45.47 5,594.12 06/27113 47.75 46.92 5,593.33 09/27113 48.54 47.71 5,591.92 12/20/13 49.95 49.12 5,591.85 03/27114 50.02 49.19 5,590.49 06/25/14 51.38 50.55 5,589.64 09/25/14 52.23 51.40 5,589.42 12/17/14 52.45 51.62 5,589.17 03/26/15 52.70 51.87 Water Levels and Data over Time White Mesa Mill -Well TWN -6 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,663.03 5,664.94 1.91 135 5,589.52 08/25/09 75.42 73.51 5,589.46 09/22/09 75.48 73.57 5,589.61 11/03/09 75.33 73.42 5,589.92 12114/09 75.02 73.11 5,590.24 03/11110 74.70 72.79 5,590.40 05/11/10 74.54 72.63 5,590.24 09/29/10 74.70 72.79 5,590.49 12/21110 74.45 72.54 5,590.16 02/28/11 74.78 72.87 5,590.44 06/21111 74.50 72.59 5,590.35 09/20/11 74.59 72.68 5,590.67 12/21/11 74.27 72.36 5,590.34 03/27112 74.60 72.69 5,590.32 06/28/12 74.62 72.71 5,589.77 09/27112 75.17 73.26 5,589.67 12/28/12 75.27 73.36 5,589.45 03/28113 75.49 73.58 5,589.01 06/27/13 75.93 74.02 5,588.99 09/27/13 75.95 74.04 5,588.15 12/20113 76.79 74.88 5,588.50 03/27/14 76.44 74.53 5,588.03 06/25114 76.91 75.00 5,587.74 09/25/14 77.20 75.29 5,587.69 12/17/14 77.25 75.34 5,587.29 03/26/15 77.65 75.74 Water Levels and Data over Time White Mesa Mill -Well TWN -7 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5,647.39 5,649.26 1.87 120 5,552.56 08/25/09 96.70 94.83 5,558.34 09/21109 90.92 89.05 5,558.82 11110/09 90.44 88.57 5,558.96 12/14/09 90.30 88.43 5,559.54 03/11/10 89.72 87.85 5,559.60 05111110 89.66 87.79 5,559.83 09/29110 89.43 87.56 5,559.00 12/21110 90.26 88.39 5,559.68 02/28111 89.58 87.71 5,560.43 06/21/11 88.83 86.96 5,560.46 09/20/11 88.80 86.93 5,560.78 12/21111 88.48 86.61 5,560.92 03/27/12 88.34 86.47 5,560.87 06/28112 88.39 86.52 5,561.40 09/27/12 87.86 85.99 5,561.50 12/28/12 87.76 85 .89 5,562.01 03/28/13 87.25 85.38 5,562.21 06/27/13 87.05 85.18 5,562.41 09/27/13 86.85 84.98 5,562.23 12/20/13 87.03 85.16 5,562.85 03/27114 86.41 84.54 5,562.95 06/25114 86.31 84.44 5,563.06 09/25/14 86.20 84.33 5,563.21 12/17/14 86.05 84.18 5,563.33 03/26115 85.93 84.06 Water Levels and Data over Time White Mesa Mill -Well TWN -14 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5,647.80 5,649.53 1.73 135 5,586.18 11/04/09 63.35 61.62 5,586.51 12114/09 63.02 61.29 5,586.71 03111110 62.82 61.09 5,586.72 05/11/10 62.81 61.08 5,586.53 09/29/10 63.00 61.27 5,586.80 12/21110 62.73 61.00 5,586.74 02/28/11 62.79 61.06 5,586.84 06/21111 62.69 60.96 5,586.73 09/20111 62.80 61.07 5,586.98 12/21/11 62.55 60.82 5,587.07 03/27/12 62.46 60.73 5,587.10 06/28/12 62.43 60.70 5,587.07 09/27112 62.46 60.73 5,587.33 12/28112 62.20 60.47 5,587.43 03/28/13 62.10 60.37 5,587.43 06/27/13 62.10 60.37 5,587.72 09/27/13 61.81 60.08 5,587.22 12/20/13 62.31 60.58 5,587.91 03/27/14 61.62 59.89 5,587.74 06/25/14 61.79 60.06 5,587.76 09/25/14 61.77 60.04 5,587.88 12/17/14 61.65 59.92 5,587.97 03/26115 61.56 59.83 Water Levels and Data over Time White Mesa Mill-Well TWN-16 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5,651.07 5,652.70 1.63 100 5,603.34 11104/09 49.36 47.73 5,603.56 12/14/09 49.14 47.51 5,603.84 03111/10 48.86 47.23 5,604.31 05/11110 48.39 46.76 5,604.28 09/29/10 48.42 46.79 5,604.39 12/21/10 48.31 46.68 5,604.20 02/28111 48.50 46.87 5,604.55 06/21/11 48.15 46.52 5,604.74 09/20111 47.96 46.33 5,604.94 12/21111 47.76 46.13 5,604.84 03/27/12 47.86 46.23 5,604.85 06/28112 47.85 46.22 5,604.99 09/27/12 47.71 46.08 5,605.10 12/28/12 47.60 45.97 5,605.22 03/28/13 47.48 45.85 5,605.11 06/27/13 47.59 45.96 5,605.39 09/27/13 47.31 45.68 5,604.99 12/20/13 47.71 46.08 5,605.71 03/27/14 46.99 45.36 5,605.16 06/25/14 47.54 45.91 5,605.10 09/25/14 47.60 45.97 5,605.25 12/17114 47.45 45.82 5,605.04 03/26/15 47.66 46.03 Water Levels and Data over Time White Mesa Mill -Well TWN -18 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5,643.95 5,645.45 1.50 100 5,586.85 11102/09 58.60 57.10 5,600.14 12/14/09 45.31 43.81 5,587.36 03/11/10 58.09 56.59 5,587.71 05/11110 57.74 56.24 5,587.50 09/29/10 57.95 56.45 5,607.66 12/21/10 37.79 36.29 5,587.35 02/28/11 58.10 56.60 5,587.71 06/21/11 57 .74 56.24 5,587.65 09/20/11 57 .80 56.30 5,587.95 12/21111 57.50 56.00 5,587.05 03/27/12 58.40 56.90 5,587.05 06/28/12 58.40 56.90 5,587.50 09/27/12 57.95 56.45 5,587.50 12/28/12 57 .95 56.45 5,587.32 03/28113 58.13 56.63 5,586.95 06/27/13 58.50 57.00 5,587.02 09/27/13 58.43 56.93 5,586.26 12/20/13 59.19 57.69 5,586.87 03/27114 58.58 57.08 5,586.23 06/25114 59.22 57.72 5,586.02 09/25/14 59.43 57.93 5,585.99 12/17114 59.46 57.96 5,585.66 03/26/15 59.79 58.29 Water Levels and Data over Time White Mesa Mill-Well TWN-19 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5,659.59 5,661.36 1.77 110 5,606.17 11/02/09 55.19 53.42 5,606.70 12/14/09 54.66 52.89 5,607.22 03111/10 54.14 52.37 5,607.89 05/11/10 53.47 51.70 5,607.98 09/29/10 53.38 51.61 5,608.41 12/21/10 52.95 51.18 5,608.49 02/28111 52.87 51.10 5,608.60 06/21111 52.76 50.99 5,609.17 09/20/11 52.19 50.42 5,608.90 12/21111 52.46 50.69 5,608.87 03/27/12 52.49 50.72 5,608.86 06/28112 52.50 50.73 5,608.86 09/27112 52.50 50.73 5,608.86 12/28/12 52.50 50.73 5,609.17 03/28/13 52.19 50.42 5,608.88 06/27/13 52.48 50.71 5,608.92 09/27113 52.44 50.67 5,608.46 12/20113 52.90 51.13 5,608.88 03/27/14 52.48 50.71 5,608.33 06/25/14 53.03 51.26 5,608.11 09/25114 53.25 51.48 5,608.36 12/17114 53.00 51.23 5,607.96 03/26/15 53.40 51.63 Water Levels and Data over Time White Mesa Mill -Well MW -30 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,613.34 5,614.50 1.16 110 5,534.92 10/24/2006 79.58 78.42 5,535.09 3/16/2007 79.41 78.25 5,535.46 8/27/2007 79.04 77.88 5,535.06 10/15/2007 79.44 78.28 5,535.78 3/15/2008 78.72 77.56 5,536.26 6/15/2008 78.24 77.08 5,536.35 9115/2008 78.15 76.99 5,536.68 11115/2008 77.82 76.66 5,535.42 3115/2009 79.08 77.92 5,537.11 6/30/2009 77.39 76.23 5,536.93 9110/2009 77.57 76.41 5,537.23 12/11/2009 77.27 76.11 5,537.59 311112010 76.91 75 .75 5,537.85 5/11/2010 76.65 75.49 5,538.37 9/29/2010 76.13 74.97 5537.70 12/2112010 76.8 75 .64 5537.67 2/28/2011 76.83 75.67 5538.31 6/2112011 76.19 75.03 5538.15 9/20/2011 76.35 75 .19 5538.42 12/21/2011 76.08 74.92 5538.54 3/27/2012 75.96 74.8 5538.60 6/28/2012 75.9 74.74 5538.68 9/27/2012 75.82 74.66 5538.99 12/28/2012 75.51 74.35 5539.25 3/28/2013 75.25 74.09 5539.05 6/27/2013 75.45 74.29 5539.60 9/27/2013 74.90 73.74 5539.67 12/20/2013 74.83 73 .67 5539.77 3/27/2014 74.73 73.57 5539.40 6/25/2014 75.10 73.94 5539.19 9/25/2014 75.31 74.15 5539.30 12117/2014 75.20 74.04 5539.01 3/26/2015 75.49 74.33 Water Levels and Data over Time White Mesa Mill-Well MW-31 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,615.26 5,616.40 1.14 130 5,544.07 10/24/2006 72.33 71.19 5,544.45 3116/2007 71.95 70.81 5,536.94 8/27/2007 79.46 78.32 5,544.62 10/15/2007 71.78 70.64 5,545.37 3115/2008 71.03 69.89 5,544.50 6/15/2008 71.90 70.76 5,545.94 9/15/2008 70.46 69.32 5,546.42 11115/2008 69.98 68.84 5,546.03 3115/2009 70.37 69.23 5,546.65 6/30/2009 69.75 68.61 5,546.45 9/10/2009 69.95 68.81 5,546.75 12111/2009 69.65 68.51 5,547.09 3/1112010 69.31 68.17 5,547.41 5/1112010 68.99 67.85 5,547.28 9/29/2010 69.12 67.98 5547.45 12/2112010 68.95 67.81 5547.37 2/28/2011 69.03 67.89 5547.96 6/2112011 68.44 67.3 5547.65 9/20/2011 68.75 67.61 5548.34 12/21/2011 68.06 66.92 5548.30 3/27/2012 68.10 66.96 5548.40 6/28/2012 68.00 66.86 5548.59 9/27/2012 67.81 66.67 5548.91 12/28/2012 67.49 66.35 5549.14 3/28/2013 67.26 66.12 5548.90 6/27/2013 67.50 66.36 5549.25 9/27/2013 67.15 66.01 5549.16 12/20/2013 67.24 66.10 5548.95 3/27/2014 67.45 66.31 5548.60 6/25/2014 67.80 66.66 5548.19 9/25/2014 68.21 67.07 5548.25 12117/2014 68.15 67.01 5548.14 3/26/2015 68.26 67.12 TabG Laboratory Analytical Reports 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. 1st Quarter Nitrate 2015 150234 7-009 Client Sample ID: Piez-01_02182015 Collection Date: 2118/2015 857h Received Date: 2/20/2015 1 045h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 2/25/2015 1853h 3/4/2015 1415h Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual E300.0 10.0 55.9 E353.2 0.100 6.41 Report Date: 3/1112015 Page 12 of 19 All analyses applicable to lhe CWA, SDWA, and RCRA are perronned in accordance 10 NELAC protocols Per1inent sampling informalion is located on the altached COC. Confidential Business lnfonnation: This report is provided for the exclusive use of Lhe addressee Privileges of subsequent use of the name of this company or any member ofils staff, or reproduction oftbis report in connection with the advertisement., promotion or sale of any product or process. or in connection wilh tile re·publication of this repot1 for any purpose oaher lhao for the addressee will be gmnled only on cont.acl This company accepls no responsibility except for Lhe due perfonnance ofinspeclion and/or analysis in good faith and according to lhe rules oflbe trade and of science. INORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. 1st Quarter Nitrate 2015 1502347-010 Client Sample ID: Piez-02_02182015 ANALvr;c., LABoRATORIEs Collection Date: 2/18/2015 835h 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Received Date: 2/20/2015 1 045h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Contact: Garrin Palmer Date Method Reporting Analytical Analyzed Used Limit Result Qual 2/25/2015 1910h E300.0 10.0 12.6 3/4/2015 1416h E353.2 0.0100 0.749 Report Date: 3/1112015 Page 13 of 19 All analyses applicable lo Lhe CWA, SDWA, and RCRA are perfonned in accordance to K'ELAC protocols Pertinent sampling information is localed on the alt.ached COC, Confidential Business ]nfonnalion: TI1is report is provided for the exclusive use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in cotlilecLion with the adverti~nent, promotion or sale of any product or pn>eess. or in connection with the re-publication of this report for any purpose othenhan for the addressee will be ~ranted only on conlact. This company accepts no responsibility excepl for Lhe due perfonnance of inspection and/or analysis in good faith and according l.fl Lhe rules of the Lmde and of science 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: I st Quarter Nitrate 2015 Lab Sample ID: 1502347-011 Client Sample ID: Piez-03_02182015 Collection Date: 2118/2015 845h Received Date: 2/20/2015 1045h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Chloride mg/L 2/25/2015 2000h E300.0 10.0 27.1 Nitrate/Nitrite (as N) mg/L 3/4/2015 1417h E353.2 0.0100 1.82 1-Matrix spike recove1y indicates matrix inte1jerence. The method is in control as indicated by the LCS. Report Date: 3/11/2015 Page 14 of 19 All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols Pertinenl sampling infonnation is located on the attached COC. Confidential Business rnfonnation: This report is provided for the exclusive use of the addressee. Pri\'ilegt!s of subsequent use of the name of litis company or any member of its staff, or reproduction of1his r.;oport in coonection wi1h I he advertisement, promoti011 or sale of any product or process. or in connection with lhe re-publication of this report for any purpose other than fo1 the addressee will be granted only on contact This company accepts no responsibility except for I he due perfonnance of inspection amUor analysis in good faith and according to the rules of the trnde am\ of science INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 1st Quarter Nitrate 2015 Lab Sample ID: 1502347-003 Client Sample ID: TWN-01_02182015 .,,,., vrtcAL L•aoAAroRIEs Collection Date: 2/18/2015 1325h 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Received Date: 2/20/2015 1045h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Contact: Garrin Palmer Date Method Reporting Analytical Analyzed Used Limit Result Qual 2/25/2015 1745h E300.0 10.0 27.8 3/4/2015 1357h E353.2 0.0100 1.37 Report Date: 3/ II /2015 Page 6 of 19 All Rna lyses applicable to !he CWA, SDWA, and RCRA are perfonned in accordance Lo J\'ELAC protocols Pertinenlsampling information IS located on the aUached COC,Confidential Business Jnfonnation: This report is provided for the ell: elusive use of the addressee PriYileges of subsequent use of the name of thi5 C'Ompany or aoy member of its staff, or reproduction of this report in conneclioo with the advertisement, rromotion or sale of any product or process. or iu connection wilh the re-publil'atioo of this repOrt for any purpose olher than fo1 the addressee will be granted only on conlacl This cotnp3ny accepts 110 responsibility except for the due ,-.ert"onnance of inspection and/or analysis in good faith and according to lhe rules oft he lr.lde ;:md or science. 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263 -8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 1st Quarter Nitrate 2015 Lab Sample ID: 1502347-006 Client Sample ID: TWN-02_02182015 Collection Date: 2118/2015 825h Received Date: 2/20/2015 1045h Analytical Results Date Compound Units Prepared Chloride mg!L Nitrate/Nitrite (as N) mg!L Date Analyzed 2125/2015 1819h 3/4/2015 140lh Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual E300.0 10.0 84.8 E353.2 1.00 48.6 Report Date: 3/11/2015 Page 9 of 19 All analyses opplicahle to the CWA, SDWA, and RCRA are perfonned in accordance Lo 1\ELAC protocols Peninenl sampling information is located on the aUached COC. Confidential Business Jnfonnation: This rqwrt is provided for the exclusi.,.e use of the addressee. Privileges of subsequent use of the name of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotiou or sale of ony pro duel or process. or in connection with the re-publication of this report for any purpose other than for the addr~ssee will be grnnted only oo conlilcL Tbis company accepts no responsibillty except for !he due performance of inspection and/01 analysis in good faith And according to the rules of tl1e trnde and of science. American West ANALYTICAL LARORATO~IfS 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 1st Quarter Nitrate 2015 Lab Sample ID: 1502347-005 Client Sample ID: TWN-03_02192015 Collection Date: 2119/2015 745h Received Date: 2/20/2015 1045h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 2/25/2015 1638h 314/2015 l400h Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual E300.0 100 164 E353.2 0.100 19.4 Report Date: 3/11/2015 Page 8 of 19 All analyses applicable to the CWA, SDWA, and RCRA are performed in accordance to KELAC pro1ocols Pertinent sampling infonnalion is located on the altached COC Confidential Business Jnronnation: This report is provided for the exclllSive u.se of the addressee. Privileges of subsequent use of the name of this company or any member of iL<> staff. or reproduction of lhis report in connection with I he advertisement, promotion or sale of :my product or process. or in connection \Vilh the re-publication of this report for any purpose olher than feu the addressee will be granted only oo contact. This company accepts no responsibility except for Lhe due perfonnance of inspection ~ndlor analysis in good raith and according Lo the rules of the tmde and of science. INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 1st Quarter Nitrate 2015 Lab Sample ID: 1502347-002 Client Sample ID: TWN-04_02182015 ANALvncAL LABORATORIEs Collection Date: 2/18/2015 1256h 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Received Date: 2/20/2015 1045h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Contact: Garrin Palmer Date Method Reporting Analytical Analyzed Used Limit Result Qual 2/25/2015 1729h E300.0 10.0 31.5 3/4/2015 1356h E353.2 0.0100 1.48 Report Date: 3/11/2015 Page 5 ofl9 All analyses applicable lo the CWA, SOW A, and RCRA are perfonned in accordance to KELAC protocols Pertinent sampling infonnation is located on the attached CDC Confidential Business Jnfonnation: This report is provided for the exclusive use oftbe addressee. Privileges of subsequent use of the name ofthls company or any member of its slaff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process. or in conneclion wilh the re-publication of this report For any purpose ol.her than for the addressee will be gran led only on conlacL This company accepts no responsibility except for the due perfonnance of inspection and/or analysis in good faith nod according ln the rules of the trnde and of science. 3440 South 700 West Salt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 e-mail: awal@awal-labs.com web: www.awal-1abs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 1st Quarter Nitrate 2015 Lab Sample ID: 1502347-001 Client Sample ID: TWN-07_02192015 Collection Date: 2119/2015 735h Received Date: 2/20/2015 1045h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Chloride rng/L 2/25/2015 2108h E300.0 1.00 5.58 Nitrate/Nitrite (as N) rng/L 3/4/2015 1343h E353 .2 0.0100 1.04 '@ @-High RPD due to suspected sample non-homogeneity or matrix inteiference. 1 -Matrix spike recovery indicates matrix inte1jerence. The method is in control as indicated by the LCS. ReportDate: 3/11/2015 Page4of19 All analyses applicable to lhe CWA, SOW A, and RCRA are perfonned in aC~;ordance to l\ELAC protocols Pertinent sampling inforrnalion is ktCuted on the al1ached COC Confidential Bu.,.ines.s Jnfonnation: This report ls provided for the exclusive use of the addressee. Pri\'ileges of subsequent use of the name of this company or any member of its staff, OJ reproduction of this report in connection v.:ith the advertisement, promotion or sale or any product or process. or in conneclion with the re-puhlication of this repo1 t for any purpose olher than for the acldr~ssee will be grnnted only on conlacl This company accepts no responsibility except for the due perfnnnance of inspection andim analysis in good fnilh nnd according to the rules of the Lrnde ;md ofscieoce 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 1st Quarter Nitrate 2015 Lab Sample ID: 1502347-012 Client Sample ID: TWN-07R_02182015 Collection Date: 2118/2015 1157h Received Date: 2/20/2015 1045h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 2/25/2015 214lh 3/4/2015 142lh Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual E300.0 1.00 < 1.00 E353.2 0.100 <0.100 Report Date: 3/ II /2015 Page 15 of 19 All analyses Applicable 10 the CWA. SDWA, and RCRA are perfonned in accordance Lo t\ELAC protocols.. Pertinent sampling infonnalion is located em the auached COC. Confidential Bu!'iness Infonnation: This report is provided for the exclusive use of1he addressee Privileges of subsequent use of the name of1his company or any member of its siBff, or reproduction of this repon in connection with the adverList:ment, promotion or sale of t:~ny product or proces<>. or in connection with the re-publication of Lhis report for any purpose other than for the addressee will be granted only on conlflcL This company accepts no responsibility e.'<cept ror the due perfonnance of inspection and/or analysis in gOt'>d raitb 11nd according to the rules of Lhe trnde anrl or scieHce.. American West MIA I YTIC~I. LADQ~fiHIIIIf. 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 1st Quarter Nitrate 2015 Lab Sample ID: 1502347-004 Client Sample ID: TWN-18_02182015 Collection Date: 2118/2015 1401h Received Date: 2/20/2015 1045h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 2/25/2015 1802h 314/2015 1358h Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual E300.0 10.0 73.3 E353.2 0.0100 1.00 Report Date: 3/11/2015 Page 7 of 19 All analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to 1'\ELAC protocols Pertinent sampling infonnalion is located on the attached COC Confidential Business 1nfonnaLion: This report is provided for lhe exclusive use of the addressee Privileges of stlbsequent use of the name of1his company or any member ofilS staff, or reproduction of this report in connection with the advertisemenl, promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other I han for the addressee will be gran led only on contact This company accepL<i no respollSibility excepl for the due perfonnance of inspection andfor analysis in good faith and according lo lhe rules of the trnde and of science. INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 1st Quarter Chloroform 2015 Lab Sample ID: 1503226-033 Client Sample ID: TW4-22_03092015 ANA l vr1 c•' '•ao••roAifs Collection Date: 3/9/2015 1336h 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Received Date: 3113/2015 1015h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Contact: Garrin Palmer Date Method Reporting Analytical Analyzed Used Limit Result Qual 3/17/2015 2054b E300.0 100 675 3/20/2015 175lh E353.2 10.0 69.2 Report Date: 3/26/20 15 Page 40 of 92 All onnlyscs npplicable Ill \he C\VA, SDWA, und R.CRA aro performed in BCC(lrduncc lo NELAC protocols. P1:ninent Mll1pling information i~ locQ\cd t>n lhc attached COC. Coufidcatial Ouiii1C$lnfonnl\lion: This rcpon i!> p1ovidcd forthecxclush·c usc oflhc addressee. P1 ivileg:cs ofsubsequ~tuusc oft he •>a me of thi~ comp.:~uy or ony m~nbct of its slnff. or reproduction of this repon in connection wilh the ndvcni!icmcm, promoaion or sale ornny product or process, or in connection with the ro-public:nion or tnis report ror any purpose mllcr ~hna ror the :.~ddrr.'sscc will b~ gntnlcd onl>-on conUI.cl. Thi!'i cmnpony ncccpL~ no responsibility c.X~tlJp~ for the due pcd'orrnancc of inspection oudior 11nalysis in ~ood raith and occllrding to the mlcs or the trade aud or scic:ncc. INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 1st Quarter Chloroform 2015 Lab Sample ID: 1503226-018 Client Sample ID: TW4-24_03092015 LABO RATo "H -Collection Date: 3/9/2015 1326h 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Received Date: 3/13/2015 1015h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Contact: Garrin Palmer Date Method Reporting Analytical Analyzed Used Limit Result Qual 311712015 2021h E300.0 100 944 3/2012015 1826h E353.2 10.0 34.6 Report Date: 3/26/2015 Page 25 of 92 All an" ly-ses applicoblc to the CWA, SDWA1 and RCRA arc pc1iformcd in acconiancc to NELAC protocols Pertinent sampling information is located on the au.achcd COC. ConfiJcntial Business lnfonn11tion: This rcpun i5 provided for the cxclusi\'c usc of the addressee. Privil('gtS ofsllhscq\IC!ll use of the nome of this company or nny member of its stniT, or reproduction of this report in connection with the ndvcrtiscllll.mt. promotiou or sale of nny product or procr:s:1, or in connection with the re-publication ofthi~ •epot1 for any PU'l'OSC other LhMl for Lhc uddrusscc will be gnmlcd only on conl.flcl This company ucccpl.s no responsibility cxcl!pL for Lhc dul! performance of inspection and/or nnolysis in yond faith ond uccording to the mlcs of !.he trade 1111d of scico~. American West ANA l YT ICA l lAOORATO RIE S 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. 1st Quarter Chlorofonn 2015 1503226-014 Client Sample ID: TW4-25~03092015 Collection Date: 3/9/2015 1300h Received Date: 3/13/2015 1015h Analytical Results Date Compound Units Prepared Chloride mg!L Nitrate/Nitrite (as N) mg/L Date Analyzed 3/17/2015 1930h 3/20/2015 1824h Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual E300.0 100 310 E353.2 1.00 14.4 Report Date: 3/26/2015 Page 21 of92 All analy!ii:S applicable to the CWA, SDWA, nnd RCRA arc P'' fonncd in occordallcc to NELAC prOlocols Pertinent !<iotnplina infonmHion is located on the ouuclt<:d COC. ConJidQnlill.l Ousinc:'IS1nronnnti('ln: This rtport i::; provided lbr 1.ho: extlusivc usr: of the addrc!Uce. Privileges of subsequent usc or the n:1mc oftbis company or any member of'i1s .stn!T, or reprod\Jcticm ~1f this tcport in connection with the ndvcrtiscmenl promotion or sale ofnny prod11C1 nr procr:&~, or h1 CQnn...:~tion wilh th~ rc-publicalion of this report for any purpose other ~u1n for the ~ddrcsscc will be grflntcd only on comacl Thi5 coll'lllany t~cccpt:s no rcspon:sibility cxCC[ll fllr Lbe J.uc pcrf'onnancc orinspcclion nullil1r nnnlysis in QtlUd (ailb and AtcordinQ to Lhe rul~$ <If the tmdc tUJd ofsdcn~ 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 1st Quarter Chloroform 2015 Lab Sample ID: 1503326-006 Client Sample ID: TW4-60_03172015 Collection Date: 3/17/2015 855h Received Date: 3/19/2015 945h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 3/19/2015 2315h 3/27/2015 1855h Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual E300.0 1.00 < 1.00 E353.2 0.100 < 0.100 Report Date: 3/31/20 15 Page I 0 of 25 All en:llys~s ttpplicablc to ~he CWA, SDWA. nnd RCRA arc p~rformcd in accordauce to NELAC protocols. PcrtincnlsamplinQ inftmnation is locrncd on the auachcd COC. Confidential Businc.-=.s Jnfonn;~tion: This report is provided for (he exclusive usc oftbc addre~sce. flrivilcp.:s of subsequent usc of the name oftbis company or any m®ber ofits .s;tn(f, or ~production ,,fthis report in connection with the advcrtiscmunl, promotion IJr sale of::my product or process, orin connection wilh lhc re~publication of this report for tay purpost: other than for tht:' addressee will be grunlcd ollly oo conlacL This. company accepts no responsibility except for tbe due pcrfonnancc of inspection ftndlol non lysis in good faith .:md according to the rules of the trade aod of science. American West ANALYTICAL lABORATORIES 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: I st Quarter Nitrate 2015 Lab Sample ID: 1502347-008 Client Sample ID: TWN-60_02192015 Collection Date: 2119/2015 710h Received Date: 2/20/2015 1045h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 2/25/2015 2125h 3/4/2015 1413h Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual E300.0 1.00 < 1.00 E353.2 0.100 < 0.100 Report Date: 3/11/2015 Page II of19 All analyses applicable to the CWA, SOW A, and RCRA are perfmmed in accordance to 1'\ELAC protocols. Pertinent sampling information is located on lhe altached CDC Confideulia\ Business lnfonnation: l11is report is provided forthe exclusive use of the addressee Pri,•ilege:'i of subsequent use oflhe name of this company or any member of its staff, or reproduction ofthi6 TC])()rt in connecaion wiLh the aclvertisemenL, prom01ion or sale of ony producl or process_ or in connection wilh lhe re-publication nfU1is rep<>1t for any purpose other than for the addressee will be granted only on conlacl. This company accepts no responsibility except for Lhe due perfonnance of inspection and/or analysis in good faith and according lo the rules of the trnde and of science .. American West ANALYTICAl LABORATORIFS 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 1st Quarter Nitrate 2015 Lab Sample ID: 1502347-007 Client Sample ID: TWN-65_02182015 Collection Date: 2/18/2015 1325h Received Date: 2/20/2015 1045h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 2/25/2015 1836h 3/4/2015 1412h Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual E300.0 10.0 29.0 E353.2 0.0100 1.41 Report Date: 3/11/2015 Page 10 of 19 All analyses npplicable to the CWA, SOW A, and RCRA are perfonned in accordance to "KElAC protocols Pertinent sampling infonnalion is located on the attached COC Confidential Busines.s lnfonnalion: This rqJOrt is provided for the exclusive use of the addressee Privileges uf subsequent use oF the name of this company or any member of its staff, or reproduction of this report in connection wilh Lbe advertisemenl, promotion or sale of any product nr process. orin connection with the re-puhlica1ion of this report for any purpose other than for lhe addressee will be gran led only on conlacL This company accepts no responsibility e:<cepl for lhe due perfonnance of inspection and/or analysis in good faith and according Lo Lhe rules of the Lrade and of science, 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Garrin Palmer Energy Fuels Resources, Inc. 6425 S. Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: 1st Quarter Nitrate 2015 Dear Garrin Palmer: Lab Set ID: 1502347 American West Analytical Laboratories received 12 sample(s) on 2/20/2015 for the analyses presented in the following report. American West Analytical Laboratories (AWAL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Approved by: Digitally signed by Jose G. J 0 S e G ~~~~~=Jose G. Rocha, • o=American West Analytical Laboratories, ou, R 0 c h 8 ~~~~=jose@awal-labs com. Date: 2015.03.11 15:23:24 -06'00' Laboratory Director or designee Report Date: 3/11/2015 Page I of19 All analyses applicable to the C\V A, SDWA, and RCRA are perfonned in accordance to K'ELAC protocols Pe11inent sumpling information is localed on the allached COC Confidenlil'll B~L~iness lnfonnalion: This report is provided for the exclusive use of the addressee Privileges of subsequent use oflhe name of this company or an)' Jne1nber of its slaff, or reproduction of lhis report in conneclioo with the adverlisemt!nt. promotion 01 sale of any pmducL 01 process. orin connection wilh lhe re·publication of Lhis report for any purpose other than for the addressee will be granted only em contact. This company accepts no responsibility except for the due perfonmmce of inspection and/or analysis in good faith ilnd according to the rules oflhe trnde and of science SAMPLE SUMMARY Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 1st Quarter Nitrate 2015 Lab Set ID: 1502347 Date Received: 2/20/2015 1 045h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 3440 South 700 West 1502347-001A TWN-07 02192015 2119/2015 735h Aqueous Anions, E300.0 Salt Lake City, UT 84119 1502347-001B TWN-07 02192015 2/19/2015 735h Aqueous Nitrite/Nitrate (as N), E353.2 1502347-002A TWN-04 02182015 2/18/2015 1256h Aqueous Anions, E300.0 1502347-002B TWN-04 02182015 2118/2015 1256h Aqueous Nitrite/Nitrate (as N), E353.2 Phone: (801) 263-8686 1502347-003A TWN-01 02182015 2118/2015 1325h Aqueous Anions, E300.0 Toll Free: (888) 263-8686 1502347-003B TWN-01 02182015 2118/2015 1325h Aqueous Nitrite/Nitrate (as N), E353.2 Fax: (80 1) 263-8687 1502347-004A TWN-18 02182015 2118/2015 1401h Aqueous Anions, E300.0 1502347-004B TWN-18 02182015 2118/2015 1401h Aqueous Nitrite/Nitrate (as N), E353.2 e-mail: awal@awal-labs.com 1502347-005A TWN-03_02192015 2/19/2015 745h Aqueous Anions, E300.0 1502347-005B TWN-03_02192015 2/19/2015 745h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 1502347-006A TWN-02_02182015 2/18/2015 825h Aqueous Anions, E300.0 1502347-006B TWN-02 02182015 2/18/2015 825h Aqueous Nitrite/Nitrate (as N), E353.2 1502347-00?A TWN-65_02182015 2118/2015 1325h Aqueous Anions, E300.0 Kyle F. Gross 1502347-007B TWN-65 02182015 2118/2015 1325h Aqueous Nitrite/Nitrate (as N), E353.2 Laboratory Director 1502347-008A TWN-60_02192015 2/19/2015 710h Aqueous Anions, E300.0 1502347-008B TWN-60 02192015 2119/2015 710h Aqueous Nitrite/Nitrate (as N), E353.2 Jose Rocha 1502347-009A Piez-0 1 02182015 2/18/2015 857h Aqueous Anions, E300.0 QA Officer 1502347-009B Piez-01 02182015 2/18/2015 857h Aqueous Nitrite/Nitrate (as N), E353.2 1502347-010A Piez-02 02182015 2/18/2015 835h Aqueous Anions, E300.0 1502347-010B Piez-02 _ 02182015 2118/2015 835h Aqueous Nitrite/Nitrate (as N), E353.2 1502347-011A Piez-03 02182015 2118/2015 845h Aqueous Anions, E300.0 1502347-011B Piez-03 02182015 2118/2015 845h Aqueous Nitrite/Nitrate (as N), E353.2 1502347-012A TWN-07R_02182015 2118/2015 1157h Aqueous Anions, E300.0 1502347-012B TWN-07R 02182015 2/18/2015 1157h Aqueous Nitrite/Nitrate (as N), E353.2 Report Date: 3/11/2015 Page 2 of 19 All analyses applicable to the CWA, SDWA, and RCRA are perronned in a~cordancc to 1'\ELAC protocols Pertinent sampling inrormation is located on the attached COC. Confidential Business lnfonnalion: This report is provided for the exclusive use oft he addressee Privileges of subsequent use oflhe name of this company or any memher of its staff, or reproduction of this report in conoectioo witlJ the adverti~nenl, promotion OT sale of;:my product or process. or in connection with the re-publication of Lhis report for any purpose other Lhan for !he addressee will be granted only on cnnlacl This company accepts no responsibility except for lhe due perfnnmmce of inspection and/or analysis in good faith and according to the rules of the tmde and of science ANAlYTICAl lABORATORIES 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awai-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Project: Lab SetiD: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: Energy Fuels Resources, Inc . Garrin Palmer 1st Quarter Nitrate 2015 1502347 2/20/2015 2118 & 2119/2015 Intact None Holding Time and Preservation Requirements: The analysis and preparation for the samples were performed within the method holding times. The samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exceptions: Sample ID Anal_yte QC Explanation 1502347-00lB Nitrate/Nitrite MS/MSD/RPD Sample matrix interference and suspected sample non-homogeneity or matrix interference. 1502347-0llB Nitrate/Nitrite MS/MSD Sample matrix interference Corrective Action: None required. Report Date: 3/11/2015 Page 3 of 19 All analyses applicable to the CWA, SDWA, ::mrl RCRA are perfonned in accordance to r\ELAC protocols PertiLlenl sampling infonnation is located on the aUached COC, Confidential Business Information: This r~ort is provided for Ll1e exclusive use of the atldressee. Privileges of subsequent use of the name of this COLnpany or any member of its staff, or reproduction of U1is report io connection with the advertisemenl promotion or sale of any product or process. or in connecLion with I he re-publication oftl1is report foJ any purpose other than for the addr~ee will be granted only on conlact This company accepts no responsibilily except for the due perfonnauce of inspection and/o1 analysis in good faith and according to lhe rules of the trnde and of science American West ANALYTICAl LABOAATOAIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1502347 Project: 1st Quarter Nitrate 2015 Analyte Result Lab Sample JD: LCS-R76056 Date Analyzed: Test Code: 300.0-W Chloride 4.87 Lab Sample JD: LCS-R76245 Date Analyzed: Tesl Code: N02/N03-W-353.2 Nil rate/Nitrite (as N) I 08 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Garrin Palmer Dept: we QC Type: LCS Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 02/25/2015 1319h m!ifL E300.0 0,00751 0.100 5.000 97.5 03/04/2015 1342h m!ifL E353 2 0.00833 0 0100 I 000 108 Limits 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QAOfficer RPDRef. RPD Amt %RPD Limit Qual Report Date: 3/ II /20 15 Page 16 of 19 All analyses applicable to the CWA, SDWA, and RCRA are perfi.1nned in accordance to XElAC protocols Pertinent sampling information is located on the attached COC1 Confidential Business Jnfonnation: Tl1is report is provided for the exclusive usc ofthe addressee Privileges of subsequent use of the name of this company or ally member of its staff, or reproduction ofHtis report in connection with I he advertiscmcot, promotion or sale of any product or process, or in connection with the re-publicarioll of this report for any purpose other than for the adtlrcsscc will be granted only on contact This company accepts no responsibility except for the llue performance of inspection and/or analysis in goot.l fairh and according to the rules of the trade and of science. Client: Energy Fuels Resources, Inc. Lab Set ID: 1502347 Project: I st Quarter Nitrate 2015 Analyte Result Lab Sample ID: MB-R76056 Date Analyzed: Test Code: 300.0-W Chloride <0.100 Lab Sample ID: MB-R76245 Date Analyzed: Test Code: N02/N03-W-353.2 Nilrate!Nitrite (as N) < 0.0100 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Garrin Palmer Dept: we QC Type: MBLK Reporting Amount Spike Ref. Units :viet hod MDL Limit Spiked Amount %REC 02/25/2015 1302h mg/L E300 0 0 00751 0 100 03/04/2015 1340h m!VL E353,2 0.00833 00100 Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt o/oRPD Limit Qual Report Date: 3/11/2015 Page 17 of 19 All analyses applicable to the CWA, SDWA, and RCRA are pcrfom1a.l in accordance to XELAC protocols. Pertinent sampling infonn.atioo is located on the att~chcd COC Conlidentialllusiness lnfonnation: 1 his report is provided for ~he e:o.:dush·e use of the addressee Privil.:ges of subsequent usc of the OIIITIC of this compauy or any member of its staff, or reproduction of this report in connection with the advcniscmcnt, promotion or sale of any product or process, or in connection with lhc re-publication of this report for any purpose orher than for the addressee will be granted only on contact. This company accepls no responsibility exccpl for the due pcrfomlarli:C ofin'>ped:.ion and/or analysis in good faith and aceording to the rules oflhc trade and ofs..;icncc 3440 South 700 West Salt Lake Ci1y, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www~awal-labs.com C SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 150234 7 Dept: we Project: 1st Quarter Nitrate 2015 QC Type: MS ReporHng Amount Spike Ref. Analyte Result Units Method MDL Limit Spiked Amount o;.R.Ec Lab SampleiO: 1502347-005AMS Date Analyzed: 02/25/2015 1655h Test Code: 300.0-W Chloride 651 mg/L E300 0 0.751 10.0 500.0 164 97.5 Lab Sample 10: 1502347-011~'11S Date Analyzed: 02/25/2015 2017h Test Code: 300.0-W Chloride 76.7 mg/L E300 0 0 0751 1,00 50 00 27.1 99.0 Lab Sample10: 1502347-00IBMS Date Analyzed: 03/04/2015 1353h Test Code: N02/N03-W-353.2 Nitrnte/Nitrite (as N) 3.04 mg!L E353.2 0 0833 0,100 I 000 I 04 200 Lab Sample 10: 1502347-0llBMS Dale Analyzed: 03/04/2015 1419h Test Code: N02/N03-W-353.2 Nitrnte/Nitrite (as N) 13_3 E353.2 0.0833 0.100 1.000 1.82 1,150 @-High RPD due to suspected sample non-homogeneity or matrix inte1:{erence 1-Malrix spike recove1y indicates matrix interference. The method is in control as indicated by the LCS. Limits 90-110 90 -110 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Ami %RPD Limit Qual '@ Report Date: 3/11/2015 Page 18ofl9 All analyses af'Phcablc to theCWA, SDWA, and RCRA are pcrfonnedin acconlancc to !'ElAC protocols, Pertinent sampling infonnation is located on the l!.tt!!ched COC Confidential Business lnf~mnatinn: This rcpcHt is provided for the exclusiY.! use of the addressee Privih:g~ of subsequent use of the name of this company or any member ufits smff, or reproduction of this report in connectton wit11 the adveniscment, promotion or sale of11ny product orprl)<;c:ss, or io connection with the rc-public01tioo oflhis report for 1!.0}' purpose other than for the aJtlrcsscc "ill be grnnkd unly on contact 'Ibis company !!CCCpts no rc~:ponsibility except fortbc Jue performance of inspection and/or anai}'SiK in gooJ faitl1 and accOfding to the rules oflhe rradc :md of science.. 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www awal-labs.com QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 1502347 Dept: we Project: 1st Quarter Nitrate 2015 QCType: MSD Reporting Amount Spike Ref. Analyte Result Units Method MDL Limit Spiked Amount %REC Lab Sample ID: 1502347-005AMSD Date Analyzed: 02/25/2015 1712h Test Code: 300.0-W Chloride 649 mg/L EJOO.O 0.751 10.0 500.0 164 97.0 Lab Sample ID: 1502347-0IIAMSD Date Analyzed: 02/25/2015 2034h Tesl Code: 300.0-W Chloride 76 3 mg/L EJOO 0 0 0751 I 00 50.00 27 I 98.4 Lab Sample ID: 1502347-00IBMSD Date Analyzed: 03/04/2015 1354h Test Code: N02/N03-W-353 2 Nitrate/Nitrite (as N) 2,44 mg/L E353 2 0.0833 0 100 I 000 104 140 Lab SampleiD: 1502347-0IIBMSD Dale Analyzed: 03/04/2015 1420h Test Code: N02/N03-W-353.2 Nitrate/Nitrile (as N) 12.4 mg!L EJ53 2 0 0833 0,100 1.000 1.82 1,060 @-High RPD due to suspected sample non-homogeneity or matrix interference~ 1-A1alrix spike recovel)' indicates matrix inte1ference The method is in conrrol as indicated b,v the LCS. Limits 90-110 90-110 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Ami %RPD limit 651 0.419 20 76.7 0.404 20 3,D4 21 8 10 13.3 700 10 Qual '@ Report Date: 3/11/2015 Page 19 of 19 All onalyscs applicable to tho CWA, SD\\'A, and RCRA are pcrfonncd in accordance to :"\ELAC" protocols Peninent sampliog infom1ation is located on the attached COC Confidential Businesslnformation: 1 hi~ fi!J)('IIt is pro\·idcd for the exclusive use of the addressee Privileges of subsequent use of the name of this company or ItO)' member of its srutl; or reproduction oftlt.is repmt in connection with the advcniscmcnt, promotiOn or sale ofiiO)' product or prl)l;css, or in connection with the r.:-publicarion ofth1s report tOr any purpose other tharr for the m.ltlrcsscc "ill be granted only on contact This company accepts no rcsronsibility except for the due performance of inspection and/or arwlysis in gooJ faith und according to the rules of the rradi.! n11d 1,)[ .sdcncc American West Analytical Laboratories UL Denison WORK ORDER Summary Work0rder:.1502347 Page I of2 Client: Energy Fuels Resources, Inc. Due Date: 3/3/2015 Client ID: DENlOO Contact: Garrin Palmer Project: 1st Quarter Nitrate 2015 QCLevel: III WO Type: Project Comments: PA Rush. QC 3 (Summary/No chromatograms)~ MUST report project specific DL's: Cl@ I mg!L, N02/N03 @ 0.1 mg!L. EDD-Denison & LOCUS. 4-Email Group; SAMPLES WITH AN "R" OR TWN-60 CAN NOT BE RUN BY 4500, THEY MUST BE RUN BY 300.0.; Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1502347-00IA TWN-07_02192015 211912015 0735h 212012015 t045h 300.0-W Aqueous df-cl I SEL Analyres: CL 1502347-0018 N02/N03-W-3S3.2 df ·no2/no3 I SEL Ana lyles: N03N02N I 502347-002A TWN-04_02182015 2/1812015 1256h 212012015 1045h 300.0-W Aqueous df-cl I SEL Ana lyles: CL 1502347-0028 N02/N03-W-353.2 df-no2/no3 I SEL Ana lyles: N03N02N 1502347-00JA TWN-01_02182015 2/1812015 1325h 2/20120 t 5 t 045h 300.0-W Aqueous df-cl 1 SEL Analytes: CL 1502347-0038 N02/N03-W-353.2 df-no2/no3 I SEL Ana lyles: N03N02N 1502347-004A TWN-18_02182015 2118/2015 1401h 212012015 1045b 300.0-W Aqueous df-cl I SEL Analyles: CL 1502347-0048 N02/N03-W-353.2 df-no2/no3 I SEL Analytes: N03N02N 1502347-00SA TWN-03_02192015 2/1912015 0745h 2/2012015 1045h 300.0-W Aqueous df-cl I SEL Analytes: CL 1502347-0058 N02/N03-W-353.2 df-no2/no3 I &"I.Amr/yl~r. N03N02N I502347-006A TWN-02_02182015 2/1812015 0825h 2120/2015 t04Sh 300.0-W Aqueous df-cl I SEL Analytes: CL 1502347-0068 N02/N03-W-353.2 df -no2/oo3 I SEL Ana/yles: N03N02N 1502347-007A TWN~5_02182015 2/18/2015 1325h 2120/2015 1045h 300.0-W Aqueous df-cl I SEL Ana lyles: CL 1502347-0078 N02/N03-W-353.2 df-no21noJ I SEL Ana/ytes: N03N02N 1502347-008A 1WN~0_02192015 2/19/2015 O?!Oh 2/20/2015 1045h 300.0-W Aqueous df-cl I SEL Analytes: CL Printed: 2120/20 IS FOR LABORATORY USE ONLY [fill out on page 1]: %M 0 RT 0 CNO TAT 0 aco HOK __ HO!L __ HOK ___ COG Emailed WORK ORDER Summary Work Order: 1502347 Page 2 of2 Client: Energy Fuels Resources, Inc. Due Date: 3/3/2015 Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1502347-0088 'IWN-60_()2192015 2/19/2015 0710h 2/20/2015 I 045h N02/N03-W-353.2 Aqueous df-no2'no3 I SEL Analytes: N03N02N 1502347-009A Piez-01_02182015 2/1812015 0857h 2120/2015 1045h 300.0-W Aqueous df·cl J SEL Ana lyles: CL 1502347-0098 N021N03-W-353.2 df-no2/no3 I SELAnalytes: N03N02N 1502347-0lOA Pin.-02_02182015 2/1812015 0835h 2/2012015 \045h 300.0-W Aqueous df-tl J SEL A1111/ytes: CL 1502347-0108 N02/N03-W-353.2 df-no2/no3 J SELAnalytes: N03N02N 1502347-0JIA Piez-03_02182015 2/18/2015 0845h 2/2012015 1045h 300.0-W Aqueous df-cl I ~61, AJt~I'.Y=: CL 1502347-0118 N02/N03-W-353.2 df ... oi/nn3. I SELAna/ytes: N03N02N 1502347-012A 'IWN-07R_02182015 2/18/2015 1157h 2/20/2015 1045b 300.0-W Aqueous df-cl I SEL Ana lyles: CL 1502347-0128 N02/N03-W-353.2 df-no21lm3 1 SELAnalytes: N03N02N Printed: 2/2012015 FOR LABORATORY USE ONLY (fill oul on page 1]: %M 0 RT 0 CN 0 TAT 0 QC 0 HOK __ HOI\__ HOK __ . COC Emh~L---- American West Analytical Laboratories 463 W. 3800 S Sal( Lake Cily, UT 64115 Phu '1e # (801) 263-8686 Toll Free# (BBB) 263-8686 -Fa.<#. 1601)263-8687 Email awal@aw&l-'abs com www,awal·~abs cotn Client: Energy Fuels Resourees, Jne. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Con lac\: Gartin Palmer Phone#: 1435) 678-2221 CeM#: .~~talmer@eneriYfueb.codlj KWdile(*oergyfuit&.com.; Email: dtur~nerg:fn.el.s.com Project Name: 1st Quarter Nitrate 2015 Proj6ct#: PO#: Sampler Name: Tanner Holliday Date Somp!<>ID: Samoled 1 T'Wtf·07_0:21920lS 2/19/2016 I TWN·04_021820l.S 2/18/2016 , T'Wl't-01_02182015 2/18/2015 • TWN·18_02182016 2/18/2015 ' TWN-03_02192015 2/19/2015 I TWN-02_02182016 2/18/2015 I TW'lf-66_02182016 2/18/2016 .a TWN·60_02192015 2/19/2015 t Piez.01_0218201S 2/18/2015 n Piez-02_02182015 2/18/2016 Plez-03_02182015 2/18/2015 I TWN-07R,021U015 2/18/2015 " l:"""r" Gj:J.. .;: HJ:!AA-.. z.flqho;: 1'1!-ICINIK-G-n.r":~ p.,_\...,....,--,..,,.. IZ.:SO r;.:::-·"'· .. llmc .....,,_ lj(~nqui$h00oy: ~· 1go!1tur11 , ..... PrintN,me: ltllflqi.UilildDy: c,_ Sl!}l1fllur• 1me: !.-><- CHAIN OF CUSTODY All anal~ will bo rond~,:~ udng NELAP acotlldiled methods ~nd all d11l11oMII be reported Uflog AW/>J....'s &landwd ar.alyto hM9 and reporlloo hmiiA',"'.:M.)unluZ"'!Iplleirir.allyrequost..tDlh9rw!Monthi•ChalnofCU91odysnd/ora11!1Ch!lddocuroenlalion ' AWAL lab Sample Sel # p 1 ,,. ,, I I QC Level: Tum Around Time: U."'-utNir arrangertNn<& ~vo '-:, m~F~. IOU.Om.e! I a.gnedreports~•J:-:,amllledl., .dlOpmon 3 Standard ohed~lhoyl!f\.·oiJII X Include EOO: l!b<f~!"Y'_ll ... ~¥ LOCUS UPLOAD I'?&.EJ_ -X. EXCEL Field Filler&d For: ··~ _ ....... , ·e ..... ~ Ftl' Compliance With: a NElAP • ,......,..;. .Z.-L _ .. 0 RCRA :J CWA • RMoAI~ft ........... 0 SDWA .....o.r.~ 0 ELAP/A2L.A 0' 0 NLLAP " g 0 Non-Comp~;:mce 'de-~ 0 Other: "' ~ j !2. "' II . --.-_,.,._,_' ,g ~ "' 0 -· ' ~ 0 0 Known Hazards • ·1'-<.ii!-8 -! ~ "' Time " !t & ,-0- Samoled 0 ~ 0 tl Sam le Comments -.~ ~ ,, "' . 735 l " X X 1256 2 '" X X \ooor-w .. 1325 ' " X X 1~41\Cul"'fl~ 1401 ' .. X X t1) .. -..... :-ryl'I'(M~•Il 745 ' ~ X X :'C: • '" 825 ~ .. X I X I ro-~·e "( -~ '"' 1325 ~ .. X X '· I .,_,.,..,._...,.. .{'0~· 710 ;) "' X X . ~ ' - - 857 ~ .. X X ;,_ . 835 2 lv X X ...... "Z'""~~0 ~ 845 ' w X X 1157 2 " .. X ,=:·) ~<'-Speciallnstroctions: ...... J>rintName: ~=·rrr .,_ rM• PrlniN•m11: 1:"~.€1111. ca. _/ -"-J.~,.6ks ,,.,..._L/,1. ..!:L.JS _/ ,_ /Nts- """'"""'' I :1 .. Slgnahlr11 ~rtitftn_,ll'r. !T'm• Analysis Ammonia COD Cyanide Metals N0_1 &NOJ O &G Phenols Sulfide TKN TPO Procedure: Frequency: Preservation Check Sheet Sample Set JI.J(Icn.:slon and pll Preservative I '2... 3 Lj S" G EH <2H2so. pH <2 H2-so. pH>12 NaOH pH<2HNOl pH<2H2so. y'e1 r/~ v-r v~5 ~r lt.r pH<2HCL / £H<2 H"'SO, pH>9NaOH, Zn Acetate pH <2 H_2so. pH <2 HLSO• Pour a small amount of sample in the sample lid Pour sample from Lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid 7 &--9 vet YeJ \.i• / In /1 yb lK' 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation + ... # • The sample required additional preservative upon receipt. The sample was received unpreserved The Sample was received unpreserved and therefore preserved upon receipt . The sample pH was unadjustable to a pH< 2 due to the sample matrix The sample pH was unadjustable to a pH> __ due to the sample matrix interference LabSetiD: /S 0 2.3 7') /7_ Yc5 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 e-mail: awa\@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Garrin Palmer Energy Fuels Resources, Inc. 6425 S. Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: 1st Quarter Chloroform 2015 Dear Garrin Palmer: Lab Set ID: 1503226 American West Analytical Laboratories received 37 sample(s) on 3/13/2015 for the analyses presented in the following report. American West Analytical Laboratories (AW AL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Approved by: Digitally signed by Jose G. J 0 S e G ' ~~~~~=Jose G. Rocha, • o=American West Analytical Laboratories, au, R 0 c h a.. ~~~tjose@awal-labs.com. Date: 2015.03.2711:01:24 -06'00' Laboratory Director or designee Report Date: 3/26/2015 Page I of92 All &tMiy~~fi ~pp\it:Qh\c to tb~ CWAt SDWA, nnd RC:RA urc rcrlbmtcd in tlccord!lncc to Nl;LAC protocol~. P~n.incnt stunpling lurQ[motitm is h:w:atcrJ on the au~th~d COC. Confidcll\ial Ilusincss ln(onnnlion: This report is pnwidcd f'or the c;:xchJsiv~ u~ aft he addt~ii$CQ. rrivil~~s Q( ii'tb~<Jll~nt usc of Lh~ IHHne Qr this compuny or Ill\)' member of its ~tCitT, or reproduclion M this rcpO(l ill c::om1ectiou wHh lbe ndverti&<:me:nL. prom~)tion or sale or any product or pmccs.~. or in conneotion with lhe ~publiemion M1hi.s fl:.port f\Jr any JlUrpo~c olhcr thtm fllr Lh~ llddl-csl!c::c will be gmnt(:d cmly on ~•lnlac;t This company occcplti no responsibility cxc~pl r-.>r the du~ pcrfnnnuncc ofills~ction nud/ol' IU'Inlysi:~ in QClud faith ond accnrding to th1.1 n1les of the 1radc ;1nd ol':t'ciCnC~:. SAMPLE SUMMARY American West Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer ANAl YTIC Al LAE3 0 RATORIES Project: 1st Quarter Chloroform 2015 Lab Set ID: 1503226 Date Received: 3/13/2015 1015h Lab Sample ID Client Sample ID Date CoHected Matrix Analysis 3440 South 700 West 1503226-001A TW4-03R_03102015 3/10/2015 755h Aqueous Anions, E300.0 Salt Lake City, UT 84119 1503226-001B TW4-03R 03102015 3/10/2015 755h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-001C TW4-03R_03102015 3/10/2015 755h Aqueous VOA by GC/MS Method 8260C/5030C Phone: (801) 263-8686 1503226-002A TW4-03 03112015 3/11/2015 746h Aqueous Anions, E300.0 1503226-002B TW4-03 03112015 3111/2015 746h Aqueous Nitrite/Nitrate (as N), E353.2 Toll Free: (888) 263-8686 1503226-002C TW4-03 03112015 311112015 746h Aqueous VOA by GC/MS Method Fax: (801) 263-8687 8260C/5030C e-mail: awal@awal-labs.com 1503226-003A TW4-12 03112015 3/11/2015 757h Aqueous Anions, E300.0 1503226-003B TW4-12 03112015 3111/2015 757h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 1503226-003C TW4-12 03112015 3111/2015 757h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-004A TW4-28_03112015 3/11/2015 804h Aqueous Anions, E300.0 Kyle F. Gross 1503226-004B TW4-28 03112015 3/11/2015 804h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-004C TW4-28 03112015 3/11/2015 804h Aqueous VOA by GC/MS Method Laboratory Director 8260C/5030C 1503226-005A TW4-32 03112015 3/11/2015 810h Aqueous Anions, E300.0 Jose Rocha 1503226-005B TW4-32 03112015 3/11/2015 810h Aqueous Nitrite/Nitrate (as N), E353.2 QA Officer 1503226-005C TW4-32 03112015 3111/2015 810h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-006A TW4-13 03112015 3111/2015 817h Aqueous Anions, E300.0 1503226-006B TW4-13_03112015 3111/2015 817h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-006C TW4-13_03112015 3111/2015 817h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-007 A TW4-36 03112015 3/11/2015 823h Aqueous Anions, E300.0 1503226-007B TW4-36_03112015 3/11/2015 823h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-007C TW4-36 03112015 3111/2015 823h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-008A TW4-27_03112015 3/11/2015 830h Aqueous Anions, E300.0 1503226-008B TW4-27 _03112015 3/11/2015 830h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-008C TW4-27_03112015 3/11/2015 830h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-009A TW4-30 03112015 3/11/2015 835h Aqueous Anions, E300.0 1503226-009B TW4-30 03112015 3/11/2015 835h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-009C TW4-30_03112015 3/11/2015 835h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-01 OA TW4-31_03112015 311112015 841h Aqueous Anions, E300.0 1503226-010B TW4-31 03112015 3111/2015 841h Aqueous Nitrite/Nitrate (as N), E353.2 Report Date: 3/26/2015 Page 2 of92 All ennly~"'~ oppli~~hh: to ~h~ CWA) SDWA, t'lt'ld RCRA ore p~rfonn-cd in ncC'ordont:c to NELAC proweols Pcrtincnt:;::uupling i11fonno~km is loci\ led on I he IIUr.u;hcd COC. Conlirlcn~inl l'i\l~incs~ lnfmmnlion: This report is plllvidtJd for I he exclusive Ul'lc of1l1c tlddrc~~e. Pl'tvik~-ts Qr~tlbS~\ICtl~ usc oflh~ 11\lm~ orthi.s ..:mnpany (1f tl.UY mt'mb~r ot'ils stnrr, or rcptudliCLion of lUis tepon in c()nneclion with the ncJ\'~ru~cmonl. pro1110Lion m· ~~~of any product or proccs:~, or in connection with the rc-puhlication ofdti~ rCf11111 fl~T ~ny purpn~c olh~r Lh;Ul ftn 1h~ addrlil'llitC will b1.' grnot~d only on cnutp,ct. This compony ncccpt.!; no r"~ponsibility ~xu~o~pl rLlr 1bc dt.~c p¢tlbmumc~ nr in;pccLiotl undlor nn~~ly!li~ in uQod foit.lt and according to tb1.1 n1lcs oflhc uadc 1H1d ol' sclcnc~. Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 1st Quarter Chloroform 2015 Lab Set ID: 1503226 Date Received: 3/13/2015 1015h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 1503226-01 oc TW4-31_03112015 3111 /2015 841h Aqueous VOA by GC/MS Method 3440 South 700 West 8260C/5030C 1503226-011 A TW4-34_03112015 3/1112015 847h Aqueous Anions, E300.0 Salt Lake City, UT 84119 1503226-0llB TW4-34_03112015 3/1112015 847h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-011 c TW4-34_03112015 3/11/2015 847h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-0 12A TW4-35_03112015 3/1112015 853h Aqueous Anions, E300.0 Phone: (80 I) 263-8686 1503226-0 12B TW4-35_03112015 311112015 853h Aqueous Nitrite/Nitrate (as N), E353.2 Toll Free: (888) 263-8686 1503226-012C TW4-35_03112015 3/1112015 853h Aqueous VOA by GC/MS Method Fax: (80 I) 263-8687 8260C/5030C e-mail: awal@awal-labs.com 1503226-0 13A TW4-23 03122015 3/12/2015 703h Aqueous Anions, E300.0 1503226-013B TW4-23_03122015 3/12/2015 703h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 1503226-0 13C TW4-23 03122015 3/12/2015 703h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-014A TW4-25_03092015 3/9/2015 1300h Aqueous Anions, E300.0 1503226-014B TW4-25 03092015 3/9/2015 1300h Aqueous Nitrite/Nitrate (as N), E353.2 Kyle F. Gross 1503226-0 14C TW4-25 03092015 3/9/2015 1300h Aqueous VOA by GC/MS Method Laboratory Director 8260C/5030C 1503226-015A TW4-14 03122015 3/12/2015 712h Aqueous Anions, E300.0 Jose Rocha 1503226-015B TW4-14 03122015 3112/2015 712h Aqueous Nitrite/Nitrate (as N), E353.2 QA Officer 1503226-0 15C TW4-14_03122015 3/12/2015 712h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-016A TW4-26 03122015 3/12/2015 720h Aqueous Anions, E300.0 1503226-0 16B TW4-26_03122015 3/12/2015 720h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-0 16C TW4-26_03122015 3/12/2015 720h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-017 A TW4-05 03122015 3/12/2015 728h Aqueous Anions, E300.0 1503226-0 17B TW4-05_03122015 3/12/2015 728h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-017C TW4-05_03122015 3/12/2015 728h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-0 18A TW4-24 03092015 3/9/2015 1326h Aqueous Anions, E300.0 1503226-0 18B TW4-24 03092015 3/9/2015 1326h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-0 18C TW4-24_03092015 3/9/2015 1326h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-019 A TW4-18 03122015 3/12/2015 738h Aqueous Anions, E300.0 1503226-0 19B TW4-18 03122015 3/12/2015 738h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-0 19C TW4-18 03122015 3/12/2015 738h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-020A TW4-09_03122015 3/12/2015 747h Aqueous Anions, E300.0 1503226-020B TW4-09_03122015 3/12/2015 747h Aqueous Nitrite/Nitrate (as N), E353.2 Report Date: 3/26/2015 Page3 of92 Allllulll~c~ nppli~.:.hlc 10 1hc CWA, SDWA1 n11d RCRA em:. pC'rronncd ill DC(;ordonc..: to NELAC' prmoools. P~:nincnt sampliny infonntnion i~ locn~.cd on the BI-Wlchcd COC. tonndcntiltl Businc~~ lnnmnnlion: Thi:~ rcpon i~ provid~.:d fnr the cxr:l115h~ u,;c llfthc addressee. Privile1.1c~ of.~uh:<~cqucm usc of the nom~ oft hi~ c:omp.any or un:--m~mh~:~t or ils stnll, 11r reproduction of this r~port in connection with the ndvcr1isc111~:nl.. prommion or Sllle of rmy J'lr{lduct or process, or in conn~.:~;tion with the rc-publi~IUion oflhh ro[lm1 f1n ;,~n~ purpus~ uth~r thr1u for lh~ ~ddrcssot: will b~ grnntcU only 1\n L:t)n\OCh This ~·omrany 1\t;C~ll.'i n~' ro:-sponsibility OXL:I.l).H for lbc Juc pcrform;,ncc nrin~(X'Ction illlL.IIOI' oM lysis ln good foilh end Dt:~;ording to the n1lcs of the !rude 3nd of sdcnC'l.'. Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 1st Quarter Chloroform 2015 Lab Set ID: 1503226 ANAL)ITIC AL l~BORA10RIES Date Received: 3/13/2015 1015h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 1503226-020C TVV4-09_03122015 3/12/2015 747h Aqueous VOA by GC/MS Method 3440 South 700 VVest 8260C/5030C 1503226-021A TVV4-33_03122015 3/12/2015 755h Aqueous Anions, E300.0 Salt Lake City, UT 84119 1503226-0218 TVV4-33 03122015 3/12/2015 755h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-021 c TVV4-33 03122015 3/12/2015 755h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-022A TVV4-08_03122015 3/12/2015 803h Aqueous Anions, E300.0 Phone: (80 l) 263-8686 1503226-022B TVV 4-08 _031220 15 3/12/2015 803h Aqueous Nitrite/Nitrate (as N), E353.2 Toll Free: (888) 263-8686 1503226-022C TVV4-08_03122015 3/12/2015 803h Aqueous VOA by GC/MS Method Fax: (801) 263-8687 8260C/5030C e-mail: awal@awal-labs.com 1503226-023A TVV4-21_03122015 3/12/2015 811h Aqueous Anions, E300.0 1503226-023B TVV4-21_03122015 3/12/2015 811h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 1503226-023C TVV4-21 03122015 3/12/2015 8llh Aqueous VOA by GC/MS Method 8260C/5030C 1503226-024A TVV4-29 03122015 3/12/2015 821h Aqueous Anions, E300.0 1503226-024B TVV4-29 _03122015 3/12/2015 821h Aqueous Nitrite/Nitrate (as N), E353.2 Kyle F. Gross 1503226-024C TVV4-29 03122015 3/12/2015 821h Aqueous VOA by GC/MS Method Laboratory Director 8260C/5030C 1503226-025A TVV4-16_03122015 3/12/2015 830h Aqueous Anions, E300.0 Jose Rocha 1503226-025B TVV4-16_03122015 3/12/2015 830h Aqueous Nitrite/Nitrate (as N), E353.2 QA Officer 1503226-025C TVV4-16_03122015 3/12/2015 830h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-026A TVV4-11_03092015 3/9/2015 1408h Aqueous Anions, E300.0 1503226-026B TVV4-11_03092015 3/9/2015 1408h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-026C TVV4-11_03092015 3/9/2015 1408h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-027 A TVV4-04_03092015 3/9/2015 1453h Aqueous Anions, E300.0 1503226-027B TVV4-04_03092015 3/9/2015 1453h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-027C TVV4-04_03092015 3/9/2015 1453h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-028A TVV4-01_03092015 3/9/2015 1443h Aqueous Anions, E300.0 1503226-028B TVV4-01_03092015 3/9/2015 1443h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-028C TVV4-01_03092015 3/9/2015 1443h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-029A MVV-04 03092015 3/9/2015 1437h Aqueous Anions, E300.0 1503226-029B MVV-04_03092015 3/9/2015 1437h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-029C MVV-04_03092015 3/9/2015 1437h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-030A MVV-26_03092015 3/9/2015 1400h Aqueous Anions, E300.0 1503226-030B MVV-26_03092015 3/9/2015 1400h Aqueous Nitrite/Nitrate (as N), E353.2 Report Date: 3/26/2015 Page 4 of92 All snnl>-sn ~I'IJUioh~ '" lh\l CWA, SDWA. und RCRA . pctrouttetl in ~t'~Nam:o lO NtLAC protoctlls. Pcr\incnt ~umpling mf1IT11ll.l'io,, J; ~at.cd tln tht MUlched COt ~m~&onu.a' ~~•lnas lnl\wm;uton· This ftt .. HIIa. l)flWt*t\ fhtll!ooclusi\'c ul'ic or the uddrc~see. f'ntlk~<' ur,a.t~b~cquem usc of lh~ nomc orlhl)f't'ltllplll.l.)l oJr llrly member ofhs .smtT, or rcprod\lctit.1n tlflhis report in twll\td,oi\ wrtb tl!e ndvcrtiscmont. prou •UCIU w ...,k \\CQI'!t flludun Hr 1~ or in ('\'U'I'I«1~tn '.It Ill \lk'f'C'1"'1h\•,··tion of thb repon fM "n)' purp,1w nl 1han fur the-adttn:,~cc willlx: gr~nt<•t ._,111) on contact Thi~ com~ny n<:t:qJts no rt:Sf'IOO!iibiliry cxc\!pl ftlr the.~ rfim»rrtU!c of iJl.spection rmdfor wl,t•ln "'-''IJJ fiilh Jt1d tct\MLfttw ~~ th~ ndt..'.t orthr: utMl•nd nr •th~nt~ ... Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 1st Quarter Chloroform 20 15 Lab Set ID: 1503226 A~~A LV TlC Al LADORATO RIES Date Received: 3/13/2015 1015h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 1503226-030C MW-26 03092015 3/9/2015 1400h Aqueous VOA by GC/MS Method 3440 South 700 West 8260C/5030C 1503226-031A TW4-02_03092015 3/9/2015 1427h Aqueous Anions, E300.0 Salt Lake City, UT 84119 1503226-031 B TW4-02 03092015 3/9/2015 1427h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-031C TW4-02_03092015 3/9/2015 1427h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-032A TW4-19_03092015 3/9/2015 1200h Aqueous Anions, E300.0 Phone: (80 1) 263-8686 1503226-0328 TW4-19 03092015 3/9/2015 1200h Aqueous Nitrite/Nitrate (as N), E353.2 Toll Free: (888) 263-8686 1503226-032C TW4-19 03092015 3/9/2015 1200h Aqueous VOA by GC/MS Method Fax: (801) 263-8687 8260C/5030C ' e-mail: awal@awal-labs.com 1503226-033A TW4-22_03092015 3/9/2015 1336h Aqueous Anions, E300.0 1503226-033B TW4-22_03092015 3/9/2015 1336h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 1503226-033C TW4-22 03092015 3/9/2015 1336h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-034A TW4-20 03092015 3/9/2015 1350h Aqueous Anions, E300.0 1503226-0348 TW4-20 03092015 3/9/2015 1350h Aqueous Nitrite/Nitrate (as N), E353.2 Kyle F. Gross 1503226-034C TW4-20 03092015 3/9/2015 1350h Aqueous VOA by GC/MS Method Laboratory Director 8260C/5030C 1503226-035A TW4-65_03112015 3/11/2015 810h Aqueous Anions, E300.0 Jose Rocha 1503226-0358 TW4-65_03112015 3/11/2015 810h Aqueous Nitrite/Nitrate (as N), E353.2 QA Officer 1503226-035C TW4-65 03112015 3/11/2015 810h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-036A TW4-70_03122015 3/12/2015 728h Aqueous Anions, E300.0 1503226-0368 TW4-70~03122015 3/12/2015 728h Aqueous Nitrite/Nitrate (as N), E353.2 1503226-036C TW4-70 03122015 3112/2015 728h Aqueous VOA by GC/MS Method 8260C/5030C 1503226-037 A Trip Blank 3/9/2015 Aqueous VOA by GC/MS Method 8260C/5030C Report Date: 3/26/2015 Page 5 of92 Allenaly:;c., rl.f'lplico.bktolhc CWA, SDWA, nnd RCRA art p~rf01mcd i" IH.::t:ordancc lo NELAC protocol;o;. P.;"rlincnl si\mpling infonnalion is located on the auached COC. Confid~ntial Ousinc:!ls lnfonn"tion: Thi~ rcpon is pnwid~d for the cx<.:lusivc usc ofLhc oddre!'isc:c. Privilc2t~ of:mb~Qlll!rH use of Lhe name orthis c(uup.·m)' or nny roc::mbcr of its stn!T. or reprodltction ol'lhi.~ ~rxm in connection with Lhc od'>·crtiscm..:nl, promoLion or sale llf nny producl or process, or in conn~cfion with \he rc·p\lblication ol'this r..:pon for any pU!lXl:W oLh~t lhllll ror Ill~ add.Jcs:wc will be gr11Ull!d only on \:(Intact Thi~ cmDpllll.Y ncccpL"i 110 N:Spon.!iibilil)' c>;~~pl for I be Jul! pcrlbnnaocc of inspection ;mW'or analy,is in good faith and accordiny, lo lb..: ntiC!i nf lhc !rode aud ol'scicncc. 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Garrin Palmer Project: Lab SetiD: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: 1st Quarter Chloroform 2015 1503226 3/13/2015 3/9-3/12/2015 Intact None Holding Time and Preservation Requirements: The analysis and preparation for the samples were performed within the method holding times. The samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exceptions: Sample ID Analyte QC Explanation 1503226-021B Nitrate-Nitrite (as N) MS/MSD Sample matrix interference 1503226-032B Nitrate-Nitrite (as N) MSD Sample matrix interference Corrective Action: None required. Report Date: 3/26/2015 Page 6 of 92 All onaly~~l'l npplicnhle to the CWA. SDWA, rmd RCR,.t\ a.rc p~rfonncd in ae~~~l'-tancc to NELAC ]Jrotocols. Pcnincnt Mlmpling inforrmnion i~ locntcd on the au.uchcd COC.:. Confidential Businc5s Tnfonntltion: Thi!i rcpnrt is provided fonh~ exclusive usc of the llddf~M~Q, Prtvile~cs or :mbscqul!nt use of lhc:: uomc oi'this Cflffi~ll)' or :~n:o tntmbct oriLS ~nnrr, or reprodu~tian of this Npon in connc~.:tion wllh the ndvcnisemenl, prnmmiou 01 ~le ur-nny rroduct nr procc,;.:~, or in conn.:ct-ion with lhc lC:·pu!Jiic:llil)D oi'this report for any purp()liC otb.cr lhnll ror the addressee will b-J grnut~d tJnl}' on ~onuu.:\. Thi!t. compuny ~c:c:~:pL-; ll(l rc~romibilit'j C:<i.CCpt ror the due pcl't'onnanc:c or in~pcction andlor nnllly.!i!i in good raith and nccording to Lh..:: mlcli or the trade :llld or scicnc~ .. 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Energy Fuels Resources, Inc. Garrin Palmer Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: Method: Analysis: 1st Quarter Chloroform 2015 1503226 3/13/2015 3/9-3/12/2015 Intact None SW-846 8260C/5030C Volatile Organic Compounds General Set Comments: Multiple target analytes were observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 3/26/2015 Page 7 of 92 All analyse:; llpplknblclo 1hc CWA) SDWA,Il.nd RCRA. urc pcrtm1ncd in ~c,mdtul~c lP NELAC prot(lCtl]s. Pcnin<.:nl :uullpling infonn:uion is \ocnLI!d un the au.acht,.'d COC. Confidcnlil'll Busincs~ lnfontHHion: This rcpon i:s provid~!d for Lhc cxcl~•~h·~: usc oflhc addrc~c~. pfi...,ik6ts ofsubsaquc:nt u~e oflhc nil me oftbis compan} M nny m~mbct a filii :-.!AlT. or rcfll't)duction ofllli$ ~pori in conncctio11 wtth tllc ndv~ni!Wmt.mt. promoTion 01 ~lc or:my product or process, or in conn..:..:tion wiH1 the rc-publicatinn of this r.,;port Hw any rurposc other thM fm lh(' athlrt~:~cc will h~ ~Ti'lolc~l onJy on con wet.. Thi~ compnny n~ccp1.~ no ~~pon!\ibiliLy cxc-Jp~ fl>r tbc dul! pcrlbnmmcc of inspc~Lion fludim tmalysis in good fai!.l1 ond Dccording to dli! ntlcs of lhc \lade end of science. American West ANAlYTICA.l LABORATORI ES Client: Energy Fuels Resources, Inc. Lab Set ID: 1503226 Project: 1st Quarter Chlorofonn 2015 Analyte Result Lab Sample ID: LCS-R76622 Date Analyzed: Test Code: 300.0-W Chloride 4.83 Lab Sample ID: LCS-R76625 Date Analyzed: Test Code: 300.0-W Chloride 4.84 Lab Sample ID: LCS-R76677 Date Analyzed: Test Code: 300.0-W Chloride 4.79 Lab Sample ID: LCS-R76791 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nittite (as N) 1.03 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 03/16/2015 1234h mg/L E300.0 0.00751 0.100 5.000 03/16/2015 2204h mg/L E300.0 0.00751 0.100 5.000 03/17/2015 1625h mg/L E300.0 0.00751 0.100 5.000 03/20/2015 1638h m!!IL E353.2 0.00833 0.0100 1.000 Garrin Palmer we LCS Spike Ref. Amount %REC 0 96.7 0 96.8 0 95.8 0 103 Limits 90-110 90-110 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPD Limit Qual Report Date: 3/26/20 15 Page 8 I of 92 AU analyses 3pplicable to the CWA. SDWA. and RCRA are perrormed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. Confidenrial Business lnfonnJ.tion: This 1eport is p1ovid~d fo1 the exclusive use of the ::1ddressec:. Privileges of subsl!quent use of the name ofihis company or any member of its stan: or reproduction of this repon in connection wilh the advertisement. promotion or sale of any product or process. or in connection with the re--publication of this report ror :my purpose other than for the :.~dJressee will be gnmtec.J only on contact. This ~;ompany accep1s no responsibility except for lhe due perronnancc of inspcc1ion and/or analysis in gootl railh and according lo the rul~ of the Ira de and of sci~nce. ANALYTICA L l ABORATOFI IES Client: Energy Fuels Resources, Inc. Lab Set ID: 1503226 Project: 1st Quarter Chloroform 2015 Analyte Result Lab Sample ID: MB-R76622 Date Analyzed: Test Code: 300.0-W Chloride < 0.100 Lab Sample ID: MB-R76625 Date Analyzed: Test Code: 300.0-W Chloride <0.100 Lab Sample ID: MB-R76677 Date Analyzed: Test Code: 300.0-W Chloride < 0.100 Lab Sample ID: MB-R7679l Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) < 0.0100 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801 ) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Garrin Palmer Dept: we QC Type: MBLK Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount o/oREC 03/16/2015 1217h mg/L E300.0 0.00751 0.100 03/16/2015 2147h mg/L E300.0 0.00751 0.100 03/17/2015 1608h mg/L E300.0 0.00751 0.100 03/20/2015 163 6h mg/L E353.2 0.00833 0.0100 Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt o/oRPD Limit Qual Report Date: 3/26/2015 Page 82 of 92 All analyses 3pplicable to the CWA. SDWA. and RCRA are ~rformed in accordance to NELAC prorocols. Pertinent sampling infonnation is locared on the attached COC. Confidential Business Information: This 1'eport is provided for the exclusivt! use of the <Jddressee. Privileges of subsequent use of the name of this company or any member ofits stafl: or reproduction of this report in connection with the advertisement, promotion or sale of any ptoduct or process, or in connection with the: rc-publicl1fion of this r~pmt fot any purpose othl!r than fur the adUressc:e will be gnmtcd only on contact. This company accepts no responsibility except lbr the due perlbnnancc of inspection and/or zmalysis in good faith and according to the rules of the tmde ami of science, American West ANAlYTICAl LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1503226 Project: 1st Quarter Chloroform 2015 Analyte Result Lab Sample ID: 1503226-00JAMS Date Analyzed: Test Code: 300.0-W Chlmide 99.6 Lab Sample ID: 1503226-0 l8AMS Date Analyzed: Test Code: 300.0-W Chloride 5,680 Lab Sample ID: 1503226-021AMS Date Analyzed: Test Code: 300.0-W Chloride 92.5 Lab Sample ID: 1503226-014AMS Date Analyzed: Test Code: 300.0-W Chlmide 804 Lab Sample ID: 1503226-00IBMS Date Analyzed: Test Code: N02/N03-W-353.2 -- Nitrate/Nitrite (as N) 1.03 Lab Sample ID: 1503226-011BMS Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 2.21 Lab Sample ID: 1503226-021BMS Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 3.23 Lab Sample ID: 1503226-032BMS Date Analyzed: Test Code: N02/N03-W -353.2 Nitrate/Nitrite (as N) 9.50 3440 South 700 West Salt Lake City, UT 8411 9 Phone: (80 I) 263-8686, Toll Free: (888) 263-8686, Fax: (80 I) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Garrin Palmer Reporting Units Method MDL Limit 03116/20151721h mg/L E300,0 0.0751 1.00 -03/16/2015 2238h mg/L E300.0 7.51 100 03/17/2015 237h mg/L E300.0 0.0751 1.00 03/17/2015 1947h mg/L E300.0 0.751 10.0 -03/20/20 15 1641 h mg/L E353.2 0.00833 0.0100 03/20/2015 1817h mg/L E353.2 0.0167 0.0200 03/20/2015 1827h mg/L E353.2 0.0417 0.0500 03/20/2015 1833h mg/L E353.2 0.0833 0.100 Dept: we QCType: MS Amount Spike Ref. Spiked Amount 50.00 50.6 5,000 944 50.00 44.2 500.0 310 1.000 0 1.000 1.21 1.000 1.91 1.000 8.56 %REC 98.0 94.7 96.5 98.8 103 100 132 94.0 '-Matrix spike recove1y indicates matrix intelference. The method is in control as i11dicated by the LCS. Limits 90-110 90-110 90-110 90-110 90-110 90-110 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPD Limit Qual Report Date: 3/26/20 15 Page 83 of 92 All analyses ~pplicable to the CWA. SDWA .. ~nd RCRA nre performed in accorc.hmcl! to NELAC protocols. Pc1tinent sampling infom1<1tion is located on tbe attached COC. Confidential Business Information: This tepml is pnwided for lhe cxdusiv~ use of the <tdtlressee. Privileges ofsubst:quent usc of the name of this company or any member ofics staO'. or reproduction of this 1cport in connection wilh tl'k: ttdv~rtisemcnt, promotion or sale of any pnxJuct or process, 01 in connection with the re-publicntion of this 1Cpt.lrt fiu any purpose other than tOr the alldressc::~ will be granted only on contact This company accepts no responsibility except for the due perfonmmce of inslXclion and/or ::mnlysis in gootl faith und acco1 ding 10 the rules of the I• ade and of science. 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer C SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 1503226 Dept: we Project: l st Quarter Chloroform 2015 QC Type: MSD Reporting Amount Spike Ref. RPDRef. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual Lab Sample 10: 1503226-00JAMSD Date Analyzed: 03/16/2015 175lh Test Code: 300.0-W Chloride 100 mg/L E300.0 O.o?51 1.00 50.00 50.6 99.7 90-110 99.6 0.857 20 -Lab Sample 10: 1503226-0ISAMSD Date Analyzed: 03/16/2015 2255h Test Code: 300.0-W Chloride 5,760 mg/L E300.0 7.51 100 5,000 944 96.3 90-110 5680 1.43 20 Lab Sample 10: 1503226-021AMSD Date Analyzed: 03117/2015 254h Test Code: 300.0-W Chloride 91.9 mg/L E300.0 0.0751 1.00 50.00 44.2 95.2 90-110 92.5 0.659 20 Lab Sample 10: 1503226-014AMSD Date Analyzed: 03/17/2015 2004h Test Code: 300.0-W Chloride 812 mg/L E300.0 0.751 10.0 500.0 310 100 90-110 804 0.978 20 Lab Sample 10: 1503226-00IBMSD Date Analyzed: 03/20/2015 1642h Test Code: N02/N03-W-353.2 . Nitrate/Nitrite (as N) 1.03 mg/L E353.2 0.00833 0.0100 1.000 0 103 90-110 1.03 0.777 10 Lab Sample ID: 1503226-011BMSD Date Analyzed: 03/20/2015 1819h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 2.26 mg/L E353.2 0.0167 0.0200 1.000 1.21 105 90-110 2.21 2.19 10 Lab Sample 10: 1503226-021BMSD Date Analyzed: 03/20/2015 1829h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 3.23 mg/L E353.2 0.0417 0.0500 1.000 1.91 132 90-110 3.23 0.0929 10 Lab Sample 10: 1503226-032BMSD Date Analyzed: 03/20/20 15 1834h Test Code: N02/N03-W-353.2 Nitrate/Niuite (as N) 9.70 mg/L E353.2 0.0833 0.100 1.000 8.56 114 90-110 9.5 2.12 10 1 -Matrix spike recovery indicates matrix inte1:[erence. The method is in control as indicated by the LCS. Report Date: 3/26/2015 Page 84 of 92 AJinna.lyses applicable ro the CWA. SDWA. nnd RCRA are ~formed in accord:J.ncc to NELAC pro1ocok Pe1tinent sampling inl'orrnation is located on the attacht!d COC, Confidential Business lnf01mation: This tepmt is provided fot the exclusive use oft.he n.ddressee. Privileges. of!'ubsequent U1'e of the name of this company or any membc::r of its stan: or reproduction of this report in connection with the advertisement, promotion 01 sale of any produr.:t or process, or in connr.:ction wirh the re-publica! ion of this report for any purpose otht!t than forth~ uddressee will be grnntcd only on conmct. This company ::tcct:-pls no responsibility except for the due pertbm1ance of inspection ~ndlor mmlysis in good fn.ith and accon.ling to the rules of the trade ~nd of science, American West Analytical Laboratories UL Denison WORK ORDER Summary Work Order: 1503226 Due Date: 3/24/2015 Page 1 of6 Client: Client ID: Project: Comments: Sample ID IS03226-00 I A IS03226-00 L B IS03226-00IC 1503226-002A 1503226-0028 IS03226-002C 1S03226-003A 1503226-003 8 1503226-003C 1503226-004A 1S03226-0048 IS03226-004C IS03226-00SA 1503226-0058 1S03226-005C Printed: 3/13/2015 Energy Fuels Resources, Inc. DENlOO 1st Quarter Chloroform 2015 Contact: Garrin Palmer QC Level: III WO Type: Project PA Rush. QC 3 (Summary/No chromatograms). RL of 1 ppm for Chloride and VOC and 0.1 ppm for N02/N03. Expected levels provided by client-see Jenn. J-flag what we can't meet. ElM Locus and EDD-Denison. Email Group.; Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage TW4-03R_03102015 3/I0/20IS 07SSh 3113/2015 IOISh 300.0-W Aqueous ~ df-wc 1 SEL Analytes: CL ---~ . -. ·-N02/N03-W-353.2 ~ df-no2/no3 1 SELAnalytes: N03N02N -.. 8260-W-DENlOO ---~ VOCF'ridge Test Group: 8260-W-DEN/00; #of Analytes: 4 I # ofSurr: 4 TW4-03_03112015 3111/2015 0746h 3113/20 L 5 LO ISh 300.0-W Aqueous ~ df-we ----I SEL Analytes: CL ----.. N02/N03-W-353.2 ~ df-no2/no3 --·--·· ---. I SEL Analytes: N03N02N ....... ~- 8260-W-DENIOO ~ VOCFridge Test Group: 8260-W-DEN/00; #of Analytes: 4 /# ofSurr: 4 TW4-12_03112015 3/11/20 1S 07S7h 3/13/201S I 0 ISh 300.0-W Aqueous ~ df-wc I SEL Analytes: CL 6 -· __.._ ........ N02/N03-W-353.2 ~ df-no2/no3 1 SEL Analytes: N03N02N . - 8260-W-DENIOO ~ VOCF'ridge Test Ct'Ottp! 8260-W-DENIOO; #of Analytes: 4 /# ofSurr: 4 TW4-28_03112015 3/11/2015 0804h 3/13/201S LOI5h 300.0-W Aqueous ~ df-wc I SEL Analytes: CL ·-N02/N03-W-353.2 0 df-no2/no3 -----. 1 SEL Analytes: N03N02N ... -·-~-8260-W-DENIOO VOCFridgc Test Group: 8260-W-DENJOO; #of Analytes: 4 /# ofSurr: 4 TW4-32_03112015 3/11/2015 0810h 3/13/2015 10 ISh 300.0-W Aqueous ~ df-wc I SELAnalytes: CL ---·-· N02/N03-W-353.2 ~ df-no2/no3 -1 SELAnalytes: N03N02N •• 8260-W-DENlOO ~ VOCFridge Test Group: 8260-W-DEN!OO; #of Analytes: 4 /# ofSurr: 4 3 J 3 3 .1 FOR LABORATORY USE ONLY [fill out on page 1]: %M I I RT I I CN I I TAT 1· I QC I I HOK __ _ HOK __ _ HOK__ coc Emal!ect :; /f 2 II 5 ~ WORK ORDER Summary WorkOrder: 1503226 Page 2 of6 Client: Energy Fuels Resources, Inc. Due Date: 3/24/2015 Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1503226-006A TVV4-t3_03112015 3/11/2015 0817h 3113/2015 l015h 300.0-VV Aqueous ~ df-wc I SEL Ana lyles: CL 1503226-0068 N021N03-W-353.2 ~ df-no2/no3 I SEL Analytes: N03N02N 1503226-006C 8260-VV-DENIOO ~ YOCFridge Test Group: 8260-W-DEN!OO; #of Analytes: 4/# ofSurr: 4 1503226-007 A TW4-36_03112015 3/11/2015 0823h 3/13/2015 I 0 ISh 300.0-W Aqueous ~ df-we -· .... ··-I SEL Analytes: CL ---1503226-0078 N021N03-W-353.2 ~ df-no2/no3 . -... ·-· .. ·-·--. I SEL Ana/ytes: N03N02N 1503226-007C 8260-W-DENIOO ~ VOCFridge Test Group: 8260-W-DENIOO; #of Analytes: 41# o.fSurr: 4 1503226-00SA TVV4-27_03112015 3/11/2015 0830h 3113/2015 !015h 300.0-W Aqueous 0 df-wc I SEL Analytes: CL ·----~ -·· .. . ------· . 1503226-0088 N02/N03-W-353.2 ~ df-no2/no3 ... -·····--··--·· I SEL Analytes: N03N02N . -1503226-008C 8260-W-DEN 100 ~ VOCFridge Test Group: 8260-W-DEN/00; #of Ana/ytes: 4 /# ofSurr: 4 1503226-009A TVV4-30 _ 03 I 12015 3/11/2015 0835h 3/13/2015 1015h 300.0-VV Aqueous ~ df-wc I SEL Analytes: CL --. 1503226-0098 N02/N03-W-353.2 ~ df-no2/no3 I SEL Analytes: N03N02N ---... -·. 1503226-009C 8260-W-DEN100 ~ VOCFridge Test Group: 8260-W-DEN/00; #of Analytes: 41# ofSurr: 4 1503226-{) 1 OA TW4-31_03112015 3/11/2015 0841 h 3/13/2015 lO ISh 300.0-W Aqueous ~ df-wc I SEL Ana/ytes: CL .. 1503226-0108 N02/N03-W-353.2 ~ df-no2/no3 I SEL Analytes: N03N02N -•. 1503226-0 I OC 8260-W-DEN!OO ~ VOCFridge Test Group: 8260-W-DENIOO; #of Analytes: 4 /# ofSurr: 4 1503226-011A TVV4-34_031 12015 3/11/2015 0847h 3/13/2015 l015h 300.0-VV Aqueous ~ df-wc I SEL Analytes: CL 1503226-0IIB N02/N03-W-353.2 ~ df-no2/no3 ... ··------I SEL Analytes: N03N02N .. -1503226-0 II c 8260-VV-DENlOO ~ VOCFridge Test Group: 8260-W-DENIOO: #of Analytes: 4 I # ofSurr: 4 1503226-012A TVV4-35_03112015 3/11/2015 0853h 3/13/2015 !015h 300.0-VV Aqueous VI df-we I SEL Ana lyles: CL Plinted: 3/13/2015 FOR LABORATORY USE ONLY [fill out on page 1]; %M I J RT I I CN I I TAT I I QC I I HOK ___ HOK ___ HOK ___ COC Emailed WORK ORDER Summary Work Order: 1503226 Page 3 of6 Client: Energy Fuels Resources, Inc. Due Date: 3/24/2015 Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Set Storage 1503226-0128 TW4-35_03112015 3/11/2015 0853h 3/13/2015 10 ISh N02/N03-W-353.2 Aqueous VI df-no2/no3 I SELAnalytes: N03N02N 1503226-012C 8260-W-DENIOO ~ YOC'Fridge 3 Test Group: 82611-W-DEN/00; #of Analytes: 4/# ofSurr: 4 1503226-013A TW4-23_03122015 3/12/2015 0703h 3/13/2015 10 ISh 300.0-W Aqueous ~ df-we .. I SEL Ana/ytes: CL 1503226-013 B N02/N03-W-353.2 ~ df-no2/no3 I SEL Analytes: N03N02N -. 1503226-0BC 8260-W-DENIOO ~ VOCFridge Test Group: 8260-W-DEN/00; #of Analytes: 4 /# ofSurr: 4 1503226-014A TW4-25_03092015 3/9/2015 1300h 3/13/2015 1015h 300.0-W Aqueous ~ df-we l SEL Analytes: CL ----........ 1503226-0148 N02/N03-W-353.2 . ~ df-no2/no3 4. ___ __......._ ____ --. -... -I SEL AnaZvtes: N03N02N 1503226-014C 8260-W-DENIOO ~ VOCFridge Test Group: 8260-W-DEN/00; #of Analytes: 4 1# ofSurr: 4 1503226-0 !SA TW4-14_03122015 . 3/12/2015 0712h 3/13/2015 1015h 300.0-W Aqueous ~ df-wc I SELAnalytes: CL . . . 1503226-0 15B N02/N03-W-353.2 ~ df-no2/no3 . I SELAnalytes: N03N02N 1503226-0 I SC 8260-W-DENJOO ~ VOCFridge Test Group: 8260-W-DEN/00; #of Alla/ytu; 4/# ofSurr: 4 1503226-0 16A TW4-26_03122015 3/12/20 15 0720h 3/13/2015 1015h 300.0-W Aqueous VI df -we I SEL Analytes: CL -· . -· 1503226-0168 N02/N03-W-353.2 J\/1 df-no21no3 I SELAna/ytes: N03N02N - 1503226-0 16C 8260-W-DENIOO ~ VOCFridge Test Group: 8260-W-DEN/110; #of Ana lyles: 4 1# ofSurr: 4 1503226-0I?A TW4-05_03122015 3/12/2015 0728h 3/13/2015 1015h 300.0-W Aqueous ~ df-wc I SEL Analytes: CL ---· --1503226-0 17B N02/N03-W-353.2 ~ df-no2/no3 -~ .. .. ' . -. I SEL Analytes: N03N02N 1503226-0 17C 8260-W-DENIOO ~ VOCFridge 3 Test Group: 8260-W-DENIOIJ; #of Ana/ytes: 4/# ofSurr: 4 1503226-0 18A TW4-24_03092015 3/9/2015 1326h 3/13/2015 1015h 300.0-W Aqueous VI df-we I SEL Ana(ytes: CL 1503226-0188 N02/N03-W-353.2 ~ df-no2/no3 I SELAnalytes: N03N02N Printed: 3/13/2015 FOR LABORATORY USE ONLY [fill out on page 1]: %M I I RT I CN I I TAT I I ac 1 1 HOK ___ HOK ___ HOK ___ COC Emailed WORK ORDER Summary Client: Energy Fuels Resources, Inc. Sample lD Client Sample lD Collected Date 1503226-0 18C TW4-24_03092015 3/9/2015 1326h 1503226-019A TW4-18_03122015 3/12/2015 0738h I 503226-0198 I 503226-0 19C 1503226-020A TW4-09_03l22015 3/1212015 0747h 1503226-0208 1503226-020C 1503226-021A TW4-33_03122015 3/12/20 I 5 0755h 1503226-021 8 1503226-021 c I 503226-022A TW4-08_03122015 3/12/2015 0803h 1503226-0228 1503226-022C 1503226-023A TW4-21_03122015 3/12/2015 081 lh 1503226-0238 1503226-023C I 503226-024A TW4-29 _ 03122015 3/12/2015 0821 h 1503226-0248 1503226-024C Work Order: 1503226 Due Date: 3/24/2015 Received Date Test Code Matrix Sel Storage 3/13/2015 IOJSh 8260-W-DENIOO Aqueous ~ VOCFridge Test Group: 8260-W-DEN/00; #of Analyles: 4 /# ofSurr: 4 3/13/2015 10 I 5h 300.0-W I SEL Analytes: CL N02/N03-W-353.2 I SEL Analytes: N03N02N 8260-W-DENIOO Aqueous Test Group: 8260-W-DENIOO; #of Anazvtes: 4 /# o{Surr: 4 3/ 13/20 15 10 ISh 300.0-W I SEL Ana/ytes: CL N02/N03-W-353.2 I SEL Analytes: N03N02N 8260-W-DENIOO Aqueous Test Group: 8260-W-DENI/JO; #of Analytes: 4 I# ofSurr: 4 31!3/20 15 10 I 5h 300.0-W I SEL Analytes: CL N02/N03-W-353.2 I SEL Analytes: N03N02N 8260-W-DENIOO Aqueous Test Group: 8260-W-DEN/00; #of Ana/ytes: 4 I# ofSurr: 4 3/13/2015 1015h 300.0-W I SEL Analytes: CL N02/N03-W-353.2 I SEL Analytes: N03N02N 8260-W-DENIOO AqLteous Test Group: 8260-W-DEN I 00; #of Ana/ytes: 4 I# ofSurr: 4 3/13/2015 J015h 300.0-W I SEL Analytes: CL N02/N03-W-353.2 I SEL Analytes: N03N02N 8260-W-DENIOO Aqueous Test Group: 8260-W-DEN/00; #of Analytes: 4 /# ofSurr: 4 3/13/2015 1015h 300.0-W 1 SEL Ana lyles: CL N02/N03-W-353.2 I SELAnalytes: N03N02N 8260-W-DENIOO Aqueous Test Group: 8260-W-DENIOO; #of Ana~vtes: 4 I# ofSurr: 4 df-wc 62J df-no2/no3 VOCFridge ~ df-wc ~ df-no2/no3 ~ VOCFridge df-we df-no2/no3 ~ VOCFridge ~ df-wc df-no2/no3 ~ VOCFridge [ill df ·we ~ df-no2/no3 ~ VOCFridgc ~ df-wc ~ df-no2/no3 ~ VOC£'1idge Page 4 of6 ) l 3 l 3 Printed: 3/13/2015 FORLABORATORYUSEONLY[filloutonpage1]: %M 1 I RT 1 I CN I I TAT 1.1 QC I I HOK __ _ HOK __ _ HOK___ COC Emailed,__ ___ _ WORK ORDER Summary WorkOrder: 1503226 Page 5 of6 Client: Energy Fuels Resources, Inc. Due Date: 3/24/2015 Sample 10 Client Sample 10 Collected Date Received Date Test Code Matrix Sel Storage 1503226-025A TW4-16_03122015 3/12/20 IS 0830h 3/13/2015 1015h 300.0-W Aqueous f./ I df-we I SEL Analytes: CL 1503226-0258 N02/N03-W-353.2 ~ df-no21no3 I SELAnalytes: N03N02N --. ·-1503226-025C 8260-W-DEN100 ~ VOCFridge 3 Test Group: 8260-W-DENIOO; #cf Ana/ytes: 4 /# ofSurr: 4 1503226-026A TW4-11_03092015 319120 15 1408h 3113/2015 IO!Sh 300.0-W Aqueous ~ df-we I SEL Analytes: CL 1503226-0268 N021N03-W-353.2 ~ df-no2/no3 I SEL Analytes: N03N02N 1503226-026C 8260-W-DEN 100 ~ VOCFridge 3 Test Group: 8260-W-DENIOO; #of Analytes: 4 /# ofSurr: 4 1503226-027 A TW4-04_03092015 319/2015 1453h 3/13/2015 1015h 300.0-W Aqueous ~ df-we I SEL Analytes: CL -IS03226-0278 N021N03-W-353.2 ~ df-no2/no3 . -.. ·--. 1 SEL Analytes: N03N02N . ' IS03226-027C 8260-W-DEN 100 ~ VOCFridge 'l Test Group: 8260-W-DENJOO; #of Analytes: 4 /# ofSurr: 4 1503226-028A TW4-01_03092015 3/9/201S 1443h 3/13/2015 I 0 ISh 300.0-W Aqueous ~ df-wc I SEL Ana lyles: CL 1503226-0288 N02/N03-W-353.2 ~ df-no2/no3 I SEL Analytes: N03N02N 1503226-028C 8260-W-DEN 100 !!Zl VOCFridge 1 Test Group: 8260-W-DEN/00; #of Ana/ytes: 4 I # ofSurr: 4 1503226-029A ~W-04_03092015 3/9/201S 1437h 3113/201S 1015h 300.0-W Aqueous ~ df-wc I SEL Analytes: CL -. IS03226-0298 N021N03-W-353.2 ~ df-no2/no3 1 SELAnalytes: N03N02N 1503226-029C 8260-W-DEN 100 ~ VOCFridge Test Group: 8260-W-DENIOO; #of Analytes: 4 I# ofSwr: 4 IS03226-030A ~W-26_03092015 3/9/20 15 1400h 3/13/201S 1015h 300.0-W Aqueous ~ df-we I SEL Ana/ytes: CL IS03226-030B N021N03-W-353.2 ~ ctr-no2/no3 1 SEL Analytes: N03N02N 1503226-030C 8260-W-DENIOO ~ VOCFridge Test Group: 8260-W-DEN/00; #of Ana/ytes: 4 /# ofSurr: 4 IS03226-031 A TW4-02_03092015 319/2015 1427h 3/13120 IS 10 ISh 300.0-W Aqueous ~ df -wc 1 SEL Ana/ytes: CL Printed: 3/13/2015 FOR LABORATORY USE ONLY [fill out on page 1]: %M I I RT I I CN I I TAT I I QC I I HOK ___ HOK ___ HOK ___ COC Emailed WORK ORDER Summary WorkOrder: 1503226 Page 6 of 6 Client: Energy Fuels Resources, Inc. Due Date: 3/24/2015 Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1503226-0318 TW4-02_03092015 3/9/2015 1427h 3/13/2015 1015h N02/N03-W-353.2 Aqueous VI df-no2/no3 1 SEL Ana/ytes: N03N02N 1503226-031 c 8260-W-DENIOO ~ VOCFridge Test Group: 8260-W-DEN/00; #cJ AnOI)Ites: 4 I # ofSurr: 4 1503226-032A TW4-l9_03092015 3/9/2015 J200h 3/13/2015 1015h 300.0-W Aqueous fil df-we 1 SEL Ana(vtes: CL 1503226-032 8 N02/N03-W-353.2 Vl df-no2/no3 1 SEL Analytes: N03N02N -1503226-032C 8260-W-DENIOO ill] vocr,idge J Test Group: 8260-W-DENIOO; #of Analytes: 4 I# ofSurr: 4 1503226-033A TW4-22_03092015 3/9/2015 1336h 3/13/2015 1015h 300.0-W Aqueous ~ df-wc I SEL Analytes: CL 00 1503226-0338 N02/N03-W-353.2 ~ df-no2Jno3 1 SEL Ana/ytes: N03N02N 1503226-033C 8260-W-DENIOO ~ VOCFridge 3 Test Group: 8260-W-DEN/00; #of Ana(vtes: 4 I # ofSurr: 4 1503226-034A TW4-20_03092015 3/9/2015 1350h 3/13/2015 1015h 300.0-W Aqueous ~ df-wc I SEL Analytes: CL 1503226-0348 N02/N03-W-353.2 ~ df-no2/no3 I SEL Ana/ytes: N03N02N -1503226-034C 8260-W-DENIOO ~ VOC:Fridge 3 Test Group: 8260-W-DEN/00; #of Analytes: 4 I# ofSurr: 4 1503226-035A TW4-65_03112015 3/11/2015 0810h 3/13/2015 1015h 300.0-W Aqueous ~ df-wc I SELAnalytes: CL -· 1503226-0358 N02/N03-W-353.2 ~ df-no2/no3 I SEL Ana/ytes: N03N02N 1503226-035C 8260-W-DENIOO ~ VOCFridgc 3 Test Group: 8260-W-DENIOO; #of Analytes: 4 I# ofSurr: 4 1503226-036A T\V4-70_03122015 3/12/2015 0728h 3/13/2015 1015h 300.0-W Aqueous ~ df -we I SEL Analytes: CL 1503226-0368 N02/N03-W-353.2 ~ df-no2/no3 . 1 SEL Analytes: N03N02N 1503226-036C 8260-W-DENIOO ~ VOCFJidge 3 Test Group: 82MI-W-DENJOO; #of Ana/ytes: 4 I # ofSwr: 4 1503226-037A Trip Blank 3/9/2015 3/13/2015 I 0 ISh 8260-W-DENIOO Aqueous ~ VOCFridge 3 Test Group: 8260-W-DEN/00; #of Analytes: 4 I # ofSurr: 4 Printed: 3113/2015 FOR LABORATORY USE ONLY [fill out on page 1]: %M I I RT I I CN I. I TAT I I QC I I HOK __ _ HOK __ _ HOK___ COC Emailed,__ ___ _ American West Analytical Laboratories 463 W. 3600 S. Salt Lake City. UT 84115 Phone# (801) 283-8686 Toll Free # (888) 263-t\686 Fax# (801) 26~687 Email awal@awal-labs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Contact: Garrin Palmer CHAIN OF CUSTODY All analysis vvlll be cahducted using NELAP accredited methods and all data wtll be reported using AWAL's standard analyte lists and reporting limits (~QL) unless specifically requested otherVv'ise an this Chain of Custody arKlfor attached documentation. L -QC ~evel: I Turn Around Time: Standard Unless other arrangements have been mede, signed reports wilt be emailsd by 5:00pm on the day thsy are dus, l( Include EDD: . LOCUS UPLOAD ISQJz_z_{p AWAL Lab Sample Set# Page 1 of 3 Oue Uiilit: -c- ' ,_ ...• { .lv;J '\. .-. ._-.. ~.1-~~ffi';~Yt;:~~~:~~:~ EXCEL Field Filtered For. I·~ ~ -=~··-;.::r:~r _ ..... ~Pilla;\I.;....~ •• F...t:ri'¥~ . ;' , ~------------~~:·:-~:::r7::t7~~~ For Compliance With: ·•· -':·. C.: i ~:11 ,a _ (435)678-2221 Cell#: a:piJiil'"*wu-8YfiiQta_co.,.; K'\vci.,CII@oaeru:Yfii•L:.o<>m: I Phone#: 0 NELAP ' 3f ·>r~, ~~~-~~~'~Q~ ·~ ~ ~~~ '~--~ ~i:·· h "[:._~· t~ Email: ·~~pfl!ak.com Project Name: 1st Quarter Chloroform 2015 Project#: PO#: ~ Q) Sampler Name: Tanner Holliday c ·n; "E 0 Sample 10~ Time lu Sampled I! IITW4-03R_03102015 755 lp 2 ITW4-03_03112015 746 Is 757 15 804 5 810 6 ~ Q' c:i oj a ll) "' " ~ ... 0 :s .., 0 "' 0 :::;; 0 D' 0 10 C'l ~ iO SDWA '' ~~~;~~~-.o:., '· o.<-_ "_:.. ;. liJ ELAP/A2LA • 'y · ~.'}'"!~, ;:-. 'tr · ,....; .. ·•.~-. 0 NLLAP ~· ...... .._ .-.. ~;.-·'•' 1 ". ~~~~ '::··t~·"·~; a Non-Compliance ---:;,._ •• fr,Mvo4.~· ..• -\ ~~ D Other: !&.. ~~1.:.. '• '.t _ ~ _~"" .. rt·'--... • ~~ ~ · ... \.···~~~·(7-,..s\•·".-.,:r.;._ 1------------11" '· u--~~ .... :_;;: ~. { ... ~.:·.ti-.J·~· -• .,.. ~ .,... ,r. ., l .:, ... • -~· ' 'Vi"',_ ·, •' • ."";.I Known Hazards ~. · ~ -~'".!;'!. . -•. 1 :1 •• ·I ci I <C. I Q I I I I I I I I I I & .. :"(· ~.•J:r.<:~ : :;,~ ~I ~1~1°1;;:1 I I I I I I I I I SampleComments II.;·~~· ... ·~-::?:~.- <D Iii!; ll) .. .... ~ ~ ('I ~ "' ,., - "' w -. •' . ·,,-,. _ ....... , , -I x I x I X I I I I I I I I I I II' '. ~·-."«· ,:_o; ,J:i.:JI,k':!_~~ ~_.-..,. X I X llllllllllll I ~~:,· -" ;-" ; -· ~--7 w xlxlx w X w X w -::::::· : : : : -~~~~:r~ I I I II rx~l X I I I \ I I I I I I ll":i,~~~~ -'}:·~-.. .· X~ X I I I i 1 I I I I I lk.~:;·~~·:·. :~-·~.: .':~. ·· .. ... r!IPP . ""'~-· ~r-"-.. 817 s w I X I X I X - 823 s w X I X I X 830 6 w I x I x I x I I I I I I I I I I II ;"J ;,,_, ~ .~ <:~""'~ >.'::--_, X I X I X ·, ~.I .,~f · ..... 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IR&C&ivad by: PitS: lsi nature Special instructions: 1'<\nl r<omo. &o...c-1-IA V.l.o.(VVIif nm~ l~o 'rlniO' IP''"' '"'"'"' wa~odl¥ lnnt~ Fecelv~4L ~ I 7 7 r -. . . . -.... . . - 1gnature ,Sigc,atuf ~. • · -----; Time: 4 _ ---__/ !>me 3/171/ IP!t·m N&no: ~~ ~~ rime: Print Name: f<s>nqUISheo Dy: ~gnature Print Name: RefmqUished by: :srgnature Print Name: Data; rnm•: Jbata: lme: ;Rs~ved by: Signature IPnnt Name: R.acelved by: Signature Jf.r:intName: /CI/'5' f / [Oats: -lmo: Date: 1me: American West Analytical Laboratories 463 W. 3600 S. Salt Lake City, UT 84115 Phone#(801)263-8686 Toll Free# (888} 263-8686 CHAIN OF CUSTODY All e.nalysis will be conducted using NELAP acc;redlled methods and all daLe will be reported using AWAL's standard analyte lisl5 and reporting limits (POL) unless specifically requested otherwise on this Chain of CUstody and/or attached documenlallon AWAL Lab Sample Set# Page 2 of 3 Fax# (801) 263-8687 Email awal@awal-labs com www.awal-labs.com I QC ~evel: I Turn Around Time: Standard ~.~-. arrangements have been made, signed reports will be emallad by 5:00 pm on thedaylhay aredue1 Di.feU>mu1 r. -... ~ f ~~~j Client Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Contact Garrin Palmer Phone#: (435) 678-2221 Cell#: gp&lmer@enerayfueb.com; KWeinal@energyfu::e:t:f.=-.c=o::rn=;,-------- Email: dba.d:&'Gtmrqfltalii~C'Utn. Project Name: ht Quarter Chloroform 2015 I Project#: I PO#: sampler Name: ~Tran;;;;n~e;rlH~o;llmidd'a:y;;--------------------1 i( Include EDD: LOCUS UPLOAD EXCEL Field Filtered For: ~l~~~s~;fp~;-~ 'r;. :.: . ·;uU.~-::"IP;, ' ; ;,v; • ', '~.·~-.,. ~.~~ ... ~-!\.:·~. \'~-~~~~_r·""~-·~~\~ ~-.,· 1-----------l o ~-~ ·-'"~""'I 1ForComplianceWKh: ~-: j" , ~-:-"! :·; ,-.1,~ \~1 0 NELAP "'-~~ \:<""1)-( .. "•''c "'·/;,~ :· 0 RCRA _ ~-· ... ~c_~ ... :ff ~ 1 .. _/ ~~ l ~ ,· ~·-, 1· 0 CWA ~·~e.~ 0 SDWA ·.• ·.~~~;;;,j'~.-·: 1'! :'' '< D ELAPIA2LA ··~,: ,-;:~·r )1;1~ ·.' :_·~: D NLLAP -• • · £ ~--..: 0 Non-~ompliance ~~~~--~; 1-~j~~.~~J:~~:;). 0 Olher. -~ -:~o.l · ,r:r.--, . 1 1-----------ll;f:t .... =~~~~:~ ·: ~;~~:; & ··.• ... ~-.~-i:'~· I'(' TW4-25_UaU!I:.!Ul5 ,, TW4-14_03122015 /(/;;i TW4-26_03122015 11• TW4-05_03122015 tffs TW4-24_03092015 l"f' TW4-18_03122015 "1,.0 TW4-09_031220 15 ,_(a TW4-33_03l22015 ,_;J1. TW4-08_03l22015 ~ 'I'W4-21_03122015 L.tl. TW4-29_031.2201S 1. 'l r-rw4-16_03122015 :!.. ~ TW+Jl_03092015 Known Hazards (~~~-, ; .,·~-~" ~i~_-1-:-;-'' .,, y· • r r IV •• '!rl.! .. " ::-l.l!.r-:.t-.::.+--i...:;;+-t--+-+-1--+-+-l--+-~-...:;:~~~:.:.:::~~--ll,;. ~~: -~'-~~:. ··~-,.):< X X X I I I I I I 11;3"''~. -_.:.. :...: .. •• ·;< . CPQ(!~~~,..~.~.. ,·' ....... (~)~ X X x I I I I I I ll'}~:.,;,.n~~--;.,-.:y _._ ,-, .,, .. -~ ,~! .. X X X I I I I I I IL1i), ..... _..,.• . (, ,_;,. ~ :-f.; !!; • ~~~~~··:· :::.•'!, X X X I I I I II' ·~ ;. ·~1 ; '·l'+. -' .~~~ .• r._:"..; .... ~~-:-~.t·~:· _'' X X X I I I I 1 I II ·-~· ~P.I'_~'mpli! .® .. >-. """,~;.... '-.;'r ~tl'-, ~~~ "'· ·:.. i.,_ .. .,. ........ ~-4-~~ ,_ ..-._:<: X X X I I I I I I 11 .~,"'·:·.:6-(i#.~-·-..;;,.c..·~·, ,:, ~~-~t~,.._.~III1~A'--f ~-1;...., : X X X I I I I I I I ~'-.Y. ·:: ~·11·! --.. ;. ·~·<'' <'_ ~-__:, ----...• ,;-~)::., .... ---,.,~ X X X I I I I I I Ill":!'£:_.,.·~·-¥~~--· p!~~-to·:,-.:;;, -· x x x I I I I I I 11~.{,..•~' :."~rn· _ -;,~~ •'..;1 1 :t· .r-.,~·-_, ~ rt'-=..: -... 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Solll.okeClty,UT 84115 Phone# (001) 263-8666 Toll F""' H (888) 263416S6 CHAIN OF CUSTODY Allar'llllys.la Wilt be condUCt.d ullng NElAP •ccnldJIId m_.hod• •nd all d.l ... will bo reporttld ualnu AWAL"a •tandard er'llllytellsll and raporl!rtg linirb {PQL\ urtou ~ly 1equU\td oUlDNMe on lhla Chail\ ol Cu:UodV llndlot &UacNd Mocum..ufion. AWAL lab Somplo Sel # P;ge l ol l L~~ Fax# (001)263-0087 Email owal@awol-lab~""" I QCLevol: I TurnAroundTIITKl: "" .. '''""'"'.,..m""'""""tooo-gjl~,~-· J!. ::""'~,:~'1-'f. :~~~ . ilt)nadrllt)OftswilbumdDdby5.00...,._. ~~ ~· .,....~ ~ _, WYJW.awal-labs.com 3 Standard lhact.ythlyarad\.111 !~~~~ .fl<".~; .... ;,g Cllant Eaer&J' Fuel& Reaource•, I11c. X lr)dud8EDQ. ~-Y~, A<lcbn: 6425 S, Bwy. 191 ~:UPLOAD ;~~~m· .-;:: ···;-~~ Blau.U..r;, UT 84611 Fleldfllliredfor. ~-·.::.c.~. ~,(,. . .:;iJ ·""i't~~-· · 'r{,';, ~ ; Jl C0f$10!: Garrln Palmcn :: .. 2..~~'' /'.~lo:r.., ForCompllon<:oWlth: • __ ..,...,-1>1~ ~~';, Phone#: (43SJ67S..2221 Ceffll: D NELAP I"W~ . =.· ~· .~-cl':'o;l_ Emall: -..n ... ~ 0 CWA !:•,~~""J::.,...., •. um;i;_ o-li7fu&l&:_ •om: Ki'olii~,."'l)''iiiOL="'l IJ RCF!A ).l\'~-l:il:. ~ .. --~ ··:j- ProloctN•me: llltQuart:uCbloroform20lS 0' g ~aA2LA ~~-:7~.::·--:~~.:\J_:':.. •.. ~.~-~-~--· Projoctlf. ~ 0 !? Nun-Compliance ~~-~-~ _ ·.~ •• ~ .. '1\\~ '_\, ;...~ ., g ~ o Olller: . , .. ~'rot~~ ,~ POll: S il !!l, B ~ ~,;1?~~7!11 Sompler Nlflle: Tanner HoUiday ~ " g o ~ ~ • ..J ~~ . ,_~11:1'--::; z Si ~ Known Hazards ~·+~ n.o:ij\~ .;-.4~ •'· Dale Time 8 f Oi :t. ~ & ~ tr<ll.i"~ 'i"~'!i ;tO:~;· 0 E 0 ..... 0 ~ -·-··-".,.._;-rf. ~ ~~ '~.!... '-SilmpleiO; Sampled Samjllad ~ ~ :z: u ;> San""eCof111T1onts . ~:'Q:,._ ~~-~~~ ~J .., TW'l.o4_0309:2015 3/9/2015 1453 s W X X X , .'~ 10.·· ,iJ._f j ~1,.03092015 3/9/2015 1443 s W X X X 'ij~Wa,""'":'~~ ~--------------------------r-----;-----i-~~~r-+-+-;--r-r-+-;--J--~r-------------11~~~~~~~~·., "( IIW-44_0309'201.5 3/9/2015 1437 5 W X X X ~~~~:'··~, ;?"-:r~·>~t.'!lrf:. ·~I 1---------------------4----4----l--+-+--l--,f--+-+-if--+-+-+--f-+-+--+-----------lll~~rh . , ·. · ~ .. ~ d IIW-26_03092015 3/9/2015 1400 s W X X X ~. :.q! ~"'-~•""-~' ;'!';,~~ ~ TW4-0Z.03092015 3/9{2015 1427 s W X X . X ~ , ::-:~/-~ ~~~ 1. T\114-19_03092016 3/9/2015 1200 li W X X X ~~~~:·. .~J ) TW4-22 .. 03092015 3/9/2015 1336 5 W X X• X ~.~~ ~j '( TW4-20.0;J092015 3/9/2015 1350 5 W X X X , \'!f ..:;c::.e~· ·~ ~] 'S TW4-65_03112016 3/11{2015 810 5 W X X X .,. . 1• ~ • ~;!< c. TW4-70.03J:i20J.S 3/12{2015 728 5 W X X X . ,-ty~ _,~~-(:~ ··: '•. ~ I· ~X .;gil~~,!)>'~~ 1 Trip Bbualt 3/9/2015 3 W X '. ·i:-_ , ~. ,§.,;"'·!~.: '·~ t-----------------------iJ-----+----tH-1--J-+--+-t-r-+--+-t-l-+--t--+-----------lli _..-.,. .. -;"' · ·"' 11 Temp Bialik ~ '"~ ;,., ;·, ' · '' 1-------------+---i------l-l--l----l--t--l--t--t--t--+--!--!--!--!--+-------llll . . · · :. "" I ' 11, • d ._.:..__. ' ~ ~=~""""'G----.~ .,."J.(I 'Z..{tS ::::.~r. "•' Spl!dW inslrucUcns; _ • ._,.. _&ti<-r,_~ ,....._ ·~c... I..............: fll""i' 1 zoo "'"'""""' .r """'' 1~ ... "1'\ Qolo< .__.., .9 '. _ -//. / .,.,.., 'l. , /' /.' .,.-See the_ Analytical Scope of Worlt for Reporting Llrnils ond VOC ll'o""iUO• _,. "'"'CJ A.§'.Lc. ~-.-'?? -? ' -/ Malytc h•t. ... ..,,_ l"rro\ol "~"'',..... £ ~~ ,t,l_~... 7 / 11mc. 'Off ~~.... """' ·--~ , 7 .,.,. ~· lb\ICUI4 .~ Tlt~-jlim .. l'rW. f4iwa-)o'ltlojl uoma ~a-A _Vole. =-.,. ""'~ fimc· nma: ~·-_, ..... Analysis Ammonia COD Cyanide Metals N02&N03 O&G Phenols Sulfide TKN TP04 Procedure: Frequency: Preservation Check Sheet s lc Set Ext Preservative I 2 J Lj r G .... pH <2 H2S04 pH <2 H2S04 pH>l2 NaOH pH<2 HN03 pH <2 H2S04 '(e-'> ~s yc5 Vc5 VcJ (..{~ pH <2 HCL If , II II II j/ pH <2 H2S04 pH> 9NaOH, Zn Acetate pH <2 H2S04 pH <2 H2S04 Pour a small amount of sample in the sample lid Pour sample from Lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid I {c5 doH 1? 1 ~s lif.5 / I 16 II Yer Ve5 I, / 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + ... # • The sample required additional preservative upon receipt. The sample was received unpreserved The Sample was received unpreserved and therefore preserved upon receipt. "The sample pH was unadjustable to a pH < 2 due to the sample matrix The sample pH was unadjustable to a pH > __ due to the sample matrix interference h .. «k.s 17 Lab Set ID: /j /~ 15 J .5 a .3 L -z-(Q '" 7__, /(J /) I~ Ycf \kS ~ v-~ I Vel J~·5 I' II I/ ]I v - I Analysis Ammonia con· Cyanide Metals N02&N03 O&G Phenols Sulfide TKN TP04 I Procedure: Frequency: Preservation Check Sheet s lc Set Ext, -- Preservative 11 20 2..{ .zz... .t~ ?...t( pH<2 H2S04 pH<2 H2S04 pH>12 NaOH pH<2HN03 pH <2 H2S04 _'{___e-') y'cs _&5 Jtc5 Yc5 t.fs pH<2HCL If , 1/ I/ II II pH<2H2S04 pH>9NaOH, ZnAcetate pH<2 H2S04 pH <2 H2S04 Pour a small amount of sample in the sample lid Pour sample from Lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid l.."r (c5 -dnH .z<D 2..'1 ~~ l.ks I I 2Y ]._i:f ~r v'e5 IT I/ 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + • # • The sample required additional preservative upon receipt. The sample was received unpreserved The Sample was received unpreserved and therefore preserved upon receipt. The sample pH was unadjustable to a pH < 2 due to the sample matrix The sample pH was unadjustable to a pH > __ due to the sample matrix interference Lab SetiD: ;.:ra3z.:z .. --u v(l- 3.1 Jl )z_ }J 'Sf )>) 3>G J ~.s Ycf \~S lh v~ 1\/# L-f--1 I/ II I/ I/ I" I/ ~ 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Garrin Palmer Energy Fuels Resources, Inc. 6425 S. Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: 1st Quarter Chloroform 2015 Dear Garrin Palmer: Lab Set ID: 1503326 American West Analytical Laboratories received 7 sample(s) on 3119/2015 for the analyses presented in the following report. American West Analytical Laboratories (AW AL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Approved by: Kyle Gross Laboratory Director or designee Report Date: 3/31/2015 Pagel of25 All an11.lys~ npplicnbk \othc CWA, SDWA, rutd RCRA 11rc pcrfo1med in uccordancc to NELAC prot()(:ol:\ Pertinent ~~unpling inf~,;~nmlion is l~o.H:d on the t\Uuclcl COC. Confidcntio.IOusincs:; lnf\lnmtion: This 1qkl(\ is rrovidtd fer \he a.clusi,:"C u:sc oftlu; addressee. Privile~;,-cs ofsubse(juem usc or the name of 1bis company or any member ofit.s .unrr, or rcptoduclion of this rcpon in connection with the tu:tvcniscmanl, prolttotion or sale oftmy product or p~--esoo. arin coonoc:\ioo. 'Wilh the: tc'-poMieltion ofllris t'tp()rt for ony PUillOSC other thl\11 for the addressee will be grontc:d only on c:ootpct. Thi~ company Rtc:cpts no rcspon$ibi1ity except for the due: pcrfonnaoce of inspection nudlur 1\Mlysis ln good fai1h iWd according to !he ruJ~ of the tr.ttk ond. ofscitore. SAMPLE SUMMARY Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 1st Quarter Chloroform 2015 Lab Set ID: 1503326 Date Received: 3/19/2015 945h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 3440 South 700 West 1503326-00lA TW 4-06R 03172015 3/17/2 015 930h Aqueous Aruons, E300.0 Salt Lake City, UT 84119 1503326-00lB TW4-06R 03172015 3/17/2015 930h Aqueous Nitrite/Nitrate (as N), E353.2 1503326-001 c TW4-06R_03172015 3/17/2015 930h Aqueous VOA by GC/MS Method 8260C/5030C Phone: (801) 263-8686 1503326-002A MW-32_03172015 3/17/2015 1400h Aqueous Aruons, E300.0 1503326-0028 MW-32_03172015 3/17/2015 1400h Aqueous Nitrite/Nitrate (as N), E353 .2 Toll Free: (888) 263-8686 1503326-002C MW-32_03172015 3/17/2015 1400h Aqueous VOA by GC/MS Method Fax: (801) 263-8687 8260C/5030C e-mail: awal@awal-labs.com 1503326-003A TW4-06 03182015 3/18/2015 757h Aqueous Aruons, E300.0 1503326-0038 TW4-06_03182015 3/18/2015 757h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 1503326-003C TW4-06_03182015 3/18/2015 757h Aqueous VOA by GC/MS Method 8260C/5030C 1503326-004A TW4-07_03182015 3/18/2015 805h Aqueous Aruons, E300.0 Kyle F. Gross 1503326-0048 TW4-07 03182015 3/18/2015 805h Aqueous Nitrite/Nitrate (as N), E353.2 1503326-004C TW4-07_03182015 3/18/2015 805h Aqueous VOA by GC/MS Method Laboratory Director 8260C/5030C 1503326-005A TW4-10 03182015 3/18/2015 812h Aqueous Aruons, E300.0 Jose Rocha 1503326-0058 TW4-10 03182015 3/18/2015 812h Aqueous Nitrite/Nitrate (as N), E353.2 QA Officer 1503326-005C TW4-10 03182015 3/18/2015 812h Aqueous VOA by GC/MS Method 8260C/5030C 1503326-006A TW4-60_03172015 3/17/2015 855h Aqueous Aruons, E300.0 1503326-0068 TW4-60 03172015 3/17/2015 855h Aqueous Nitrite/Nitrate (as N), E353.2 1503326-006C TW4-60_03172015 3/17/2015 855h Aqueous VOA by GC/MS Method 8260C/5030C 1503326-007 A Trip Blank 3117/2015 Aqueous VOA by GC/MS Method 8260C/5030C Report Date: 3/31/2015 Page2 of25 All .,,I .... OJ'f!lEOohlc IO lhC CWA, SOW A..,., RCRI\ Ill< f""(OI11led in O<tonlancc"' ELM~ proW(od t<11<0<rn ;omplins '"'"""'""'" n·t.l<nood on <he at<ochod coc. (.'on!ikllwl ~ lnfm•o>l•n Thl; """'I f'tUvlcl<,tl\>rll><> <lltlu•l\cusc or <he oddrnlllli::Ct rn~l<"..r-. .... Qf. ubscqucm usc of tht td1'n;' nl'UII' tm~'lY'"' any mcmbel' or tl.t.biT. Arn'Tfl\4U .. Unu ofllUt rcpon in ('Ott\acttinn Wlillthc odvcrtisct~t.:llt., prou'flb'\tlfl w. s:~ko<~t:-"~ ~~tut1 (II~'-.:"$$.."' m \"00~ \\10 ~ 1\ ... .(l®f~ll~ oflhis r-:::pm\ for .All}' rmrm . ~lll-;rtt LliD.q for the add~sscc '"'~II ~ ,OtiiiU d 1\l'll)'.t'ln [fllnlD.Cl. Tllis comp. rl}' IJQCI:JU't no h:-(\OQliblh~ ~Xpl for' l'b: l~fJJ.f''PCC ofinsp.zctmn (lll(l/OrQnC.\J3lt'fl ~, fllihh.a~ t«t·~·dmw ~ tt~ ualtt tlr~tottc M~ 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Garrin Palmer Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: 1st Quarter Chloroform 2015 1503326 3/19/2015 3117-3/19/2015 Intact None Holding Time and Preservation Requirements: The analysis and preparation for the samples were performed within the method holding times. The samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exceptions: te Nitrate-Nitrite (as N) Corrective Action: None required. Report Date: 3/31/2015 Page 3 of 25 All ann lyse::; applicable to the CWA, SDWA, nnd RCRA urc pcrrunncd in nccordAnct lo NELAC protocols, Pcrtincntsompling in[onnation is locntcd on lhc anucbcd COC. Conildcminl Business lnflm,lnlion: Thb T~m is provided for the exclusive use of the addressee. Privileges of subsequent use ofLhc ne.m~ of this comprmy or ony member or its 1\ICilT. or repl'oduclion oflbis report in connccUon whh the adveniscment, promotion or 58k ofoRy producl or pf\'K."'CSS. twiu coo:ncclion wilh 1h.: n;.pub~knlion oflhis t'l!pott for eny purpose olhcr lhar:1 (or lhc addn:sscc will be gro.ntcd only on coolo.cl-. This compo.ny Rcccpts no rcsponsibilily except for lhc due pcrfonnance ofinspcclion onJ!or o.n11lys.i~ in good i'aHh and lll..::oocdiU}}. to lbc lUlcs oflbc l.t8do o.ud Qfsdcntc, 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Energy Fuels Resources, Inc. Garrin Palmer Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: Method: Analysis: 1st Quarter Chloroform 2015 1503326 3/19/2015 3/17-3/19/2015 Intact None SW-846 8260C/5030C Volatile Organic Compounds General Set Comments: Multiple target analytes were observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date; 3/31/2015 Page 4 of 25 Alluo;~lyscs llpplicnblc to the CWA, SDWA, nnd RCRA arc performed in accordnncc to NELAC protocols Pcnincnl sampling infunnation is localcd on the auachcd COC. Con6dl;fl\i41 Busin~"i lnibfmntion: This n:pon is provided for lb<! cxclusin:~ usc oflhc addressee .. Privileges ofsl•bs~uent use of1hc name of this ccnnp~my or any member ofils sU1IT, or rcp\'Oduction of this r~port in connection with the ndvcniscmenL, prommion l11 snle oro.ny pn.'<tuc.:lorproce.s:., orin cotlucctiun with the re-.publknlian t)fthis 1'¢pcm for r~ny purpose olhcr th11.n for tb~ llddrcsscc will be gr:mtcd only on contacL this Clllllpnny ut:ccpts no rcsponsibilily cx~cpl n.)J the due pcrfonmmcc of inspct:Liou nnd/or nMlysis in~ f!ilb and IH."Cording to lh~ :rules of the trade aud of ~citnet:. Client: Energy Fuels Resources, Inc. Lab Set ID: 1503326 Project: lst Quarter Chloroform 2015 Analyte Result Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 I) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Garrin Palmer Dept: we Method MDL Reporting Limit QC Type: LCS Amount Spiked Spike Ref. Amount %REC Lab Sample ID: LCS-R76798 DateAnalyzed: 03/19/20151755h Test Code: 300.0-W Chloride Lab Sample ID: LCS N03-R77035 Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 4.87 mg/L E300.0 Date Analyzed: 03/27/2015 1732h 1.05 mg/L E353.2 0.00751 0.100 5.000 0 97.4 0.00833 0.0100 1.000 0 105 Limits 90-110 90. 110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 3/31/2015 Page 18 of 25 AIJ analyses applicable to the CWA, SDWA. and RCRA are performed in accordance ro NELAC protocols. Perrin~nt sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addre::-see. Privileges of subsequent use of the name of this company or ~my member of its stafT, or reproduction of this report in connl!ction with the advertisement, promotion 01· sale of any product or process, or in connection with the 1 e-publication of this •eport for any purpose olhe!t than for the uddressl!t! will be granted only on contm;t, This company accepts no resllonsibility except for the due p~rfonnance of inspection and/or nnalysis in good faith cmd according to the rules of the tmde and of science. Client: Energy Fuels Resources, Inc. Lab Set ID: 1503326 Project: 1st Quarter Chloroform 2015 Analyte Result Lab Sample 10: MB-R76798 Date Analyzed: Test Code: 300.0-W Chloride <0.100 Lab Sample 10: MB-R77035 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) < 0.0100 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 1) 263-8686, Toll Free: (888) 263-8686, Fax: (80 1) 263-8687 e-mail: awal@awa1-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Garrin Palmer Dept: we QC Type: MBLK Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 03/19/2015 1738h mg/L E300.0 0.00751 0.100 -03/27/2015 1729h n~IL E353.2 0.00833 0.0100 Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPD Limit Qual Report Date: 3/31/20 15 Page 19 of 25 AIJ analyses applicable to the CWA. SDWA, and RCRA are performed in accordance ro NELAC protocols. Pertinent sampling in10rmation is located on rbe attached COC Confidential Business Information: This report is provided for the exclusive use of the uddressee. Privileses of subsequent use of'l·h!! name of this com puny or nJ'ly member of its stan~ or reproduction of this report in r.::onnection with the advertisement, promotion or sale of any p1 otluct or process, or in connection with the re-publication of this n:port for any purpo~e othe1 than for the uddress.ee will be grnntt:d only on contact, This company accepts no responsibility except for the due performance of inspection anlVor analysis in good faith and according to tbe rules of the trade and of science. Client: Energy Fuels Resources, Inc. Lab Set ID: 1503326 Project: 1st Quarter Chlorofonn 2015 Analyte Result Lab Sample ID: 1503326-002AMS Date Analyzed: Test Code: 300.0-W Chloride 84.9 Lab Sample ID: 1503326-00IBMS N03 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.06 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (80 I) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Garrin Palmer Dept: we QC Type: MS Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 03/19/2015 2134h mg/L E300.0 0.0751 1.00 50.00 36.3 97.3 -03/27/2015 1847h mg/L E353.2 0.00833 0.0100 1.000 0 106 Limits 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPD Limit Qual Report Date: 3/31 /2015 Page 20 of 25 All analyses applicable to the CWA. SDWA, nnU RCRA are performed in accordance to NELAC protocols. Pe1iinent stlmpling information is located on the attached COC. Confidential BusinfsS Information: This report is provided for the exclusive use of lhe addressee. Privileges ofsubseqlll:~l1t ust: of the name of this company or any rnem~r of irs staff, or reproduction of this report in connection with the advertisement, promotion or s<Jle of any product or process, 01 in connection with the !'~·publication of this 1eport fot• any purpose otlle1 than for the addressee will be grunted only on contnct. This company accepts no responsibility except for the dLJe performance of inspection ~nd/or analysis in good faith cu1d according to the rules of the trade and of science. Client: Energy Fuels Resources, Inc. Lab Set ID: 1503326 Project: 1st Quarter Chloroform 2015 Analyte Result Lab Sample ID: 1503326-002AMSD Date Analyzed: Test Code: 300.0-W Chloride 84.2 Lab Sample ID: 1503326-00lBMSD N03 Date Analyzed: Test Code: N02/N03-W-353.2 Nin11te/Nitrite (as N) 1.11 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (80 I) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Garrin Palmer Dept: we QCType: MSD Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 03/19/2015 2151h mg/L E300.0 0.0751 1.00 50.00 36.3 95.7 -03/27/2015 1849h mg/L E353.2 0.00833 0.0100 1.000 0 Ill 1-Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Limits 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPD Limit 84.9 0.905 20 1.06 4.53 10 Qual Report Date: 3/31 /20 15 Page 21 of 25 All analyses applicable to the CWA. SDWA, and RCRA. are perfonned in accordance to NELAC prutocols. Pertinent sampling information is located on the auached COC. Conftdemial Businl!ss lnfom1ation: This report is provided for the exclusive use ofthe addressee. Privilege.." of subsequent use of the name of this company or any member of irs staff, or r~production of this report in connection with the advertis~ment, promotion 01 sale of any product or process, or in conn~ction wirh the re-publication of this report f01 nny purpose other than fo1 the addrt:ssee will be gnmted only on contm:t. This company accepts no responsibility except tbr the due perfonnance ofinspectioo and/or analysis in good fHith arid according to the rules of the trade a11tl of science American West Analytical Laboratories UL Den~on WORK ORDER Summary Work Order: 1503326 Due Date: 3/30/2015 Page 1 of2 Client: Client ID: Project: Comments: Sample II> 1503326-001A 1503326-001B 1503326-00IC 1503326-002A l503326-002B 1503326-002C 1503326-003A 1503326-00JB 1503326-00JC 1503326-004A 1503326-004B 1503326-004C 1503326-005A 1503326-005B 1503326-005C Printed: 3/19/2015 Energy Fuels Resources, Inc. DENlOO Contact: Garrin Palmer 1st Quarter Chloroform 2015 QC Level: III WO Type: Project PA Rush. QC 3 (Summary/No chromatograms). RL of 1 ppm for Chloride and VOC and 0.1 ppm for N02/N03. Expected levels provided by client-see Jenn. J-flag what we can't meet. ElM Locus and EDD-Denison. Email Group.; Client Sample II> Collected Date Received Date Test Code Matrix Sel Storage TW4-06R_03172015 3/17/2015 0930h 3/19/2015 0945h 300.0-W Aqueous df-wc 1 SEL Analytes: CL N02/N03-W-353.2 df-no2/no3 1 SEL AtiiJ!ytes: N03N02N 8260-W-DENlOO VOCFridge Test Group: 8260-W-DEN100; #of Analytes: 4 I # ofSurr: 4 ~-32_03172015 3/17/2015 1400h 3/19/2015 0945b 300.0-W Aqueous df-wc 1 SEL Analytes: CL N02/N03-W -353.2 df-no2/no3 1 SEL Analytes: N03N02N 8260-W-DEN100 VOCFridge Test Group: 8260-W-DEN100; #of Analytes: 4 I# ofSurr: 4 11¥4-06_03182015 3/18/2015 0757h 3/19/2015 0945h 300.0-W Aqueous df-wc 1 SEL Analytes: CL N02/N03-W-353.2 df -no2/no3 1 SEL Analyta.~: N03N02N 8260-W-DEN100 VOCFridge Test Group: 8260-W-DEN100; #of Analytes: 4 I# ofSurr: 4 11¥4-07_03182015 3/18/2015 0805h 3/19/2015 0945h 300.0-W Aqueous df-wc 1 SEL Analytes: CL N02/N03-W-353.2 df-no2/no3 I SEL Analytes: N03N02N 8260-W-DEN100 VOCFridge Test Group: 8260-W-DEN100; #of Analytes: 4 I # ofSurr: 4 11¥4-10_03182015 3/18/2015 0812h 3/19/2015 0945h 300.0-W Aqueous df-wc 1 SEL Analytes: CL N02/N03-W-353.2 df-no2/no3 1 SELAnalytes: N03N02N 8260-W-DEN100 VOCFridge Test Group: 8260-W-DEN100; #of Analytes: 4 1# ofSurr: 4 3 3 .. .> 3 3 FOR LABORATORY USE ONLY [fill out on page 1): %M 0 RT 0 CN 0 TAT 0 QC 0 HOK __ _ HOK __ _ HOK__ coc Emailed J /11/ti ~ WORK ORDER Summary Client: Energy Fuels Resources, Inc. Sample ID Client Sample ID 1503326-006A 1rYV4-60_03172015 1503326-006B 1503326-006C 1503326-007 A Trip Blank Collected Date Received Date Test Code 3/17/2015 0855h 3119/2015 0945h 300.0-W 1 SEL Analytes: CL N02/N03-W-353.2 1 SEL Analytes: N03N02N 8260-W-DENIOO Matrix Aqueous Work Order: 1503326 Due Date: 3/30/2015 Sel Storage df-wc df-no2/no3 VOCFridge Test Group: 8260-W-DEN100; #of Analytes: 4 /# ofSurr: 4 3/17/2015 3/19/2015 0945h 8260-W-DENlOO Aqueous VOCFridge Test Group: 8260-W-DENJ 00;· #of Analytes: 4 I# of Surr: 4 Page 2 of2 Printed: 3/19/2015 FOR LABORATORY USE ONLY [fill out on page 1]: %M 0 RT 0 CN 0 TAT 0 QC 0 HOK HOK __ _ HOK___ COC Emalled=------ CUI!NT: ADDRESS: CoNTACT: PHONE#: EMAIL: PROJECT NAME: AMERICAN WEST ANALYTICAL LABORATORIES 463 W . 3600 S. SALT LAKE CtTY. UT 84115 PHONE # (801) 263-8686 TOLL FREE # (888) 263-8686 FAX # (801) 263-8687 EMAIL AWAL@AWAL-LABS.COM WWW.AWAL-LABS.COM Energy Fuels Resources, Inc. 6425 S. Hwy. 191 Blanding, UT 84511 Garrin Palmer (4351678-2221 ce~~ #: tpa:tiDex@eiieriYfUels.comj KW:erDel@energyfu-diir-.c..,o"'m""; _______ __ d.~ 1st Quarter chloroform 2015 CHAIN OF CUSTODY /$d ~34-P ALL ANALYSIS WILL Bl! CONDUCTeD USING NELAP ACCRI!OITI!D Mi.THOOS AND AU. DATA WILL BE REPCJRTIED USING AWAL's STANDARD ANALYTe USTS AND REPORTING tAUT'S (PQL) UN1..£SS SPBCIF\CAU.Y R2QUI!STED OTMI!RWISI! ON TMIS CHAtN OF CUS1'0DV AND/oR. ATTAcHeD OOCUMI!NTATION. AWAL w~:;s:;;:;.PLE SET# PAGE OF 1-QC ~BVBL: I TURN .AROUND TIMB: STANDARD Utd•.:a:a crn::wtt ~~lQ:!:.I.Ie)m H.t.;':'l: Du.af1):;.c-1i;i. · ·""' OftN htADe. =M)NI!D RDOJnc wtlL •• ... ""-"'>IV 5;PO l'lo! 01' T>ll <MV -..-11'' ~ ~~·· .~:.~ ~ ,, -~: __ ~--~.::---AAI! 1>\1&. X INC~UDE EDD: LOCUS UPLOAD EXCEL FIELD FILTERED FoR: ' _JJ: ...... ' .·t."'~:.;.~~~~~~·k -.~ --w:~6 -~· ~.,~~.....,.:..! ~ li;·i; " ·; 8-.:~···,v-·-· ~ez"~~:~~rvx-; .-........ ~ .. -~ .. -~··· ....._--------u-2--:' .. -·-~--=. .. ·, . ' FoR COMPLIANC:B WITH: ·, . • :'. \:_'·~.:"", t•· '',0 Cl NELAP b · ~n;~~Aiul\.~ · "' > ' "'"' -occ D RCRA ~· ..:.~ ... "':.\ "-"":"~-. i. ~~ , 0 CWA ..4-,1\~J~S'R~~~•' 0 SDWA , , .''~~~~e-' '~ 0 ELAP I A2LA '' . ,y ,' · ·-; 'i; '•t 1i 0 NLLAP ;. :"'• ... -~ _ "~·~~~ ... ,:. · '~ n D NoN-COMPUANCE ~~i;,~¥-Y1'!U!"'J'·,· ~o 0 OTHER: --~ ~· ~ • ~ • ~--1£~z~::::-: .. :· -~ .4~~: KNOWN HAZARDS , 't. -~~-~~~;: J,;.. .-~·-"-, \ ~ ~ ' ...._ --~~ '1 -;~!__. .. & ~-~~. ',·><.·t ;· ..... --...... __ _ .. _ _ SAMPLE COMMENTS ~·: ,~:~ ~ ._-~: ~::e\:-; ~{~~ ~· -------------4~~~~--~~~-F~~~~;t--r-l--1--t--t--t--r-1--r---------------~~~~~~~::I~;:; .,. •'-'j\'~ ; ... JN .. , t"~ !j~. • --..... .'C,?....... ·~ • ; .. ~ ~ .. .:--. -:. -----------+~~~~~~-...;~~-~-f:....~:-+-~+~+-+-+-i-i--lr-lr-r--r'lr-------------,.--~-, ~~,..~~:=~"'1:<$P.7 · 1"-:r~.i>..iJ:-..;::C': .. ' -----------4.:~:.!.~~~-~~:..--t-t:.+-~+.::.-+~-+--t--t--t--ii-t--t--t-t-t-------------, ~~Ps~;;~~, ~: -: I I -~;-. ,q_-"i' ~· N~.· _.-d DATe: [TIMe:: DA"l"E!: triME' DATI!: ITiMI!!!: ~v~ -·~~~~____:,-. "' ~--. ;' ---~--:-~ ... . ~·il<~sr.w.a .. ~ 4-A .. ~ a.NZi,Coc-~·-~ ~ ..-.,., ··-: I. rv ..... --· , t 1 ·;\, ••• ~ r.._. ,1"-. ,, ~ ',.i · -., . ·:. · -:r.·., 2~~1:1 -~ ~ ·-:.. ~ SPE<!IAL. INSTRUCTIONS: . ,. ~ .::--""~' ~_;; .... -..O"'r Analysis Ammonia COD Cyanide Metals N02&N03 O&G Phenols Sulfide TKN TP04 Procedure: Frequency: Preservation Check Sheet -.-·· ·.------------------s le Set E Preservative l 2.-.. 0 tf .J & pH <2 H2S04 pH<2 H2 S04 pH >12 NaOH pH <2 HN03 pH <2 H2S04 VcJ ~ 1/~ v~ Ves /e~ pH <2 HCL I I pH <2 H2S04 pH >9NaOH, Zn Acetate pH <2 H2S04 pH <2 H2S04 Pour a smnll nmount of sample in the sample lid Pour sample from Lid gently over wide range pH pnper Do Not clip the pH paper in the sample bottle or lid loH ··-- I 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + .... # • The sample required additional preservative upon receipt. The sample was received unpreserved The Sample was received unpreserved and therefore preserved upon receipt. The sample pH was unadjustable to a pH< 2 due to the sample matrix The sample pH was unadjnstable to a pH > __ due to the sample matrix interference Lab Set 10: IS G 3:f-t--.VJ , TabH Quality Assurance and Data Validation Tables H-1 Field Data QAJQC Evaluation Volume Location Casing Volume 2x Casing Volume Pumped Volume Check Piezometer 1 -- Piezometer 2 - Piezometer 3 -- TWN-1 33.70 67.40 88.00 OK TWN-2 NA Continuously Pumped Well TWN-3 37.28 74.56 47.60 Pumped Dry TWN-4 47.47 94.94 121.00 OK TWN-7 12.47 24.94 16.50 Pumped Dry TWN-18 55.64 111.28 132.00 OK TW4-22 NA Continuously pumped well TW4-24 NA (:onLi nu1uusly pumped well r TW4-25 NA Comi11uously pumped well NC =Not Calculated TWN-2, TW4-22, TW4-24, and TW4-25 are continuously pumping wells. Piezometers 1, 2, and 3 were not pumped, only one set of parameters were taken. TWN-3 and TWN-7 were pumped dry and sampled after recovery. CQitduc.:livity 2124 790 2764 851.0 853.0 2948 2294.0 2299.0 1063.0 1063.0 1229.0 1237.0 2250.0 2247.0 6073 7593 2891 ~~~~~~ II RPD NC NC NC 0.23 6.76 NC 0.22 6.60 0.00 6.52 0.65 6.20 0.13 6.16 NC NC NC pH }lPb Tenl_l) RPD Rt:dox Potential RPD Turbidit.y, RPb 8.93 NC 13.20 NC 193 NC 0.0 NC 6.87 NC 13.34 NC 299 NC 0.0 NC 11.23 NC 13.25 NC 148 NC 0.0 NC 6.78 0.30 15.06 15 .07 0.07 194 I 193 0.52 0.0 I 0.0 0.00 6.56 NC 14.71 NC 311 NC 0.0 NC 6.59 0.15 13.99 13.99 0.00 NM NC NM NC 6.52 0.00 14.73 14.73 0.00 224 I 224 0.00 0.0 I 0.0 0.00 6.25 0.80 13.98 14.01 0.21 NM NC NM NC 6.16 0.00 14.54 14.52 0.14 178 I 178 0.00 0.0 I 0.0 0.00 6.28 NC 15.25 NC 200 NC 0.0 NC 6.24 NC 15.61 NC 220 NC 0.0 NC 6.56 NC 15.00 NC 149 NC 0.0 NC H-2: Holding Time Evaluation Allowed Hold Time Hold Time Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) (Days) Check PIEZ-01 Chloride 02118/2015 02/25/2015 7 28 OK PIEZ-01 Nitrate/Nitrite (as N) 02118/2015 03/04/2015 14 28 OK PIEZ-02 Chloride 02118/2015 02/25/2015 7 28 OK PIEZ-02 Nitrate/Nitrite (as N) 02118/2015 03/04/2015 14 28 OK PIEZ-03 Chloride 02/18/2015 02/25/2015 7 28 OK PIEZ-03 Nitrate/Nitrite (as N) 02/18/2015 03/04/2015 14 28 OK TWN-01 Chloride 02/18/2015 02/25/2015 7 28 OK TWN-01 Nitrate/Nitrite (as N) 02/18/2015 03/04/2015 14 28 OK TWN-02 Chloride 02/18/2015 02/25/2015 7 28 OK TWN-02 Nitrate/Nitrite (as N) 02/18/2015 03/04/2015 14 28 OK TWN-03 Chloride 02/19/2015 02/25/2015 6 28 OK TWN-03 Nitrate/Nitrite (as N) 02/19/2015 03/04/2015 13 28 OK TWN-04 Chloride 02/18/2015 02/25/2015 7 28 OK TWN-04 Nitrate/Nitrite (as N) 02/18/2015 03/04/2015 14 28 OK TWN-07 Chloride 02/19/2015 02/25/2015 6 28 OK TWN-07 Nitrate/Nitrite (as N) 02/19/2015 03/04/2015 13 28 OK TWN-07R Chloride 02/18/2015 02/25/2015 7 28 OK TWN-07R Nitrate/Nitrite (as N) 02/18/2015 03/04/2015 14 28 OK TWN-18 Chloride 02/18/2015 02/25/2015 7 28 OK TWN-18 Nitrate/Nitrite (as N) 02/18/2015 03/04/2015 14 28 OK TW4-22 Chloride 03/09/2015 03/17/2015 8 28 OK TW4-22 Nitrate/Nitrite (as N) 03/09/2015 03/20/2015 11 28 OK TW4-24 Chloride 03/09/2015 03/17/2015 8 28 OK TW4-24 Nitrate/Nitrite (as N) 03/09/2015 03/20/2015 11 28 OK TW4-25 Chloride 03/09/2015 03/17/2015 8 28 OK TW4-25 Nitrate/Nitrite (as N) 03/09/2015 03/20/2015 11 28 OK TW4-60 Chloride 03/17/2015 03/19/2015 2 28 OK TW4-60 Nitrate/Nitrite (as N) 03/17/2015 03/27/2015 10 28 OK TWN-60 Chloride 02/19/2015 02/25/2015 6 28 OK TWN-60 Nitrate/Nitrite (as N) 02/19/2015 03/04/2015 13 28 OK TWN-65 Chloride 02/18/2015 02/25/2015 7 28 OK TWN-65 Nitrate/Nitrite (as N) 02/18/2015 03/04/2015 14 28 OK H-3: Analytical Method Check Pilr~uneur ~elJi()d Method Usedh,Y'L~ Nitrate E353.1 or E353.2 E353.2 A4500-Cl B or A4500-Cl E Chloride orE300.0 E300.0 Both Nitrate and Chloride were analyzed with the correct analytical method. -eponmg H4.R! lffilt ec L' . Ch k Required Lab Reporting Reporting Dilution Location Analyte Limit Units Qualifier Limit RLCheck Factor PIEZ-01 Chloride 10 mg/L 1 OK 10 PIEZ-OI Nitrate/Nitrite (as N) O.I mg/L O.I OK IO PIEZ-02 Chloride 10 mg/L I OK IO PIEZ-02 Nitrate/Nitrite (as N) O.OI mg/L O.I OK I PIEZ-03 Chloride IO mg/L 1 OK 10 PIEZ-03 Nitrate/Nitrite (as N) 0.01 mg/L O.I OK I TWN-OI Chloride 10 mg/L I OK 10 TWN-OI Nitrate/Nitrite (as N) O.OI mg/L O.I OK I TWN-02 Chloride 10 mg/L 1 OK 10 TWN-02 Nitrate/Nitrite (as N) I mg/L O.I OK 100 TWN-03 Chloride 100 mg/L I OK 100 TWN-03 Nitrate/Nitrite (as N) O.I mg/L 0.1 OK 10 TWN-04 Chloride 10 mg/L I OK IO TWN-04 Nitrate/Nitrite (as N) O.OI mg/L O.I OK I TWN-07 Chloride 1 mg/L 1 OK 1 TWN-07 Nitrate/Nitrite (as N) 0.01 mg!L 0.1 OK 1 TWN-07R Chloride 1 mg/L u 1 OK 1 TWN-07R Nitrate/Nitrite (as N) 0.1 mg/L u 0.1 OK 1 TWN-18 Chloride 10 mg/L 1 OK IO TWN-18 Nitrate/Nitrite (as N) 0.01 mg/L 0.1 OK 1 TW4-22 Chloride 100 mg/L 1 OK 100 TW4-22 Nitrate/Nitrite (as N) 10 mg/L 0.1 OK 100 TW4-24 Chloride 100 mg/L 1 OK 100 TW4-24 Nitrate/Nitrite (as N) 10 mg/L 0.1 OK 100 TW4-25 Chloride 100 mg/L 1 OK 100 TW4-25 Nitrate/Nitrite (as N) 1 mg/L 0.1 OK 10 TW4-60 Chloride 1 mg/L u 1 OK 1 TW4-60 Nitrate/Nitrite (as N) O.I mg/L u O.I OK 1 TWN-60 Chloride 1 mg/L u I OK 1 TWN-60 Nitrate/Nitrite (as N) O.I mg/L u 0.1 OK 1 TWN-65 Chloride 10 mg/L 1 OK 10 TWN-65 Nitrate/Nitrite (as N) 0.01 mg!L 0.1 OK 1 U = Value was reported by the laboratory as nondetect. H-5 QAJQC Evaluation for Sample Duplicates H-6 QC Control Limits for Analysis and Blanks Method Blank Detections All Method Blanks for the quarter were non-detect. M.aEnX. :SDlKC 'Yo x eaoverv urn oans.0n- Lab Report Lab Sample ID Well Analyte MS %REC 1502347 1502347-011BMS Piez-03 Nitrate 1502347 1502347-001BMS TWN-07 Nitrate 1503226 1503226-021BMS TW4-33 Nitrate 1503226 1503226-032BMS TW4-19 Nitrate 1503326 1503326-001BMS TW4-06R Nitrate * -Recovery was not calculated because the analyte of the sample was greater than 4 times the spike amount N/A-QC was not performed on an EFRI sample. NC-Not calculated Laboratory Control Sample All Laboratory Control Samples were within acceptance limits for the quarter. 1150 200 132 94 106 REC MSD%REC Range RPD 1060 90-110 7.00 140 90-110 21.8 132 90-110 0.0929 114 90-110 2.12 111 90-110 4.53 H7R . T E 1 -CCeJpl cmpcn'Jlur~ va uatwn , Samwe· Batch -we~rsr:m Jhlttb Temperlfture; Piezometer 1, Piezometer 2, Piezometer 3, TWN-1 , TWN-2, 1502347 TWN-3, TWN-4, TWN-7, TWN-07R, TWN-18, TWN-60, 2.2 oc TWN-65 1503226 TW4-22, TW4-24, TW4-25, TW4-60 2.9 oc 1503326 TW4-60 3.4 °C H-8 Rinsate Evaluation All rinsate and DI blank samples were non-detect for the quarter. Tab I Kriged Current Quarter Isoconcentration Maps NS = not sampled; NO = not detected ......_ 1 0 kriged nitrate isocon and label TW4-37 temporary perched monitoring well + NS installed March, 2015 (not sampled) MW-4 perched monitoring well showing e 5.8 concentration in mg/L TW4·7 Q 4.3 TWN·1 <>1.4 PIEZ·1 ~ 6.4 temporary perched monitoring well showing concentration in mg/L temporary perched nitrate monitoring well showing concentration in mg/L perched piezometer showing concentration in mg/L TW4·35 temporary perched monitoring well ~ 0.44 installed May, 2014 showing concentration in mg/L NOTE: MW·4. MW-26, TW4-1, TW4-2, TW4-4, TW4-11 ,TW4-19; and TW4-20 are chloroform pulliplflg wel!s: TW4-22, TW4-24, TW4·25, and TWN-2 are nitrate pumping well HYDRO GEO CHEM,INC. KRIGED 1st QUARTER, 2015 NITRATE (mg/L) (NITRATE + NITRITE AS N) WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H:/718000/may15/nitrate/Unt0315_rev.srf I I -1 NS = not sampled; ND = not detected ...._ 100 kriged chloride isocon and label TW4·37 +Ns MW-4 .41 TW4-7 Q 40 TWN-1 ~28 PIEZ-1 .. 67 TW4-36 ~67 temporary perched monitoring well installed March, 2015 (not sampled) perched monitoring well showing concentration in mg/L temporary perched monitoring well showing concentration in mg/L temporary perched nitrate monitoring well showing concentration in mg/L perched piezometer showing concentration in mg/L temporary perched monitoring well installed May, 2014 showing concentration in mg/L NOTE: MW-4, MW-26, TW4-1, TW4-2, TW4-4, TW4-11 ,TW4-19, and TW4-20 are chloroform pumping wells; TW4-22, TW4-24, TW4-25, and TWN-2 are nitrate pumping we.U HYDRO GEO CHEM,INC. KRIGED 1st QUARTER, 2015 CHLORIDE (mg/L) WHITE MESA SITE APPROVED DATE REFERENCE I FIGURE H:/718000/may15/chloride/Ucl0315_rev.srf I-2 TabJ Analyte Concentrations Over Time Piezometer 1 Date Nitrate (mg/1) Chloride (mg/1) 2/19/2009 6.8 NA 7/14/2009 6.8 60 9/22/2009 7.3 78 10/27/2009 7.4 61 6/2/2010 7.2 52 7/19/2010 6.8 52 12/10/2010 6.5 60 1/31/2011 7 60 4/25/2011 6.8 58 7/25/2011 7 53 10/19/2011 6.6 55 1/11/2012 7.1 78 4/20/2012 6.6 58 7/27/2012 7.2 56 10/17/2012 7.66 55 2/18/2013 8.11 56.7 4/24/2013 8.88 53.3 8/28/2013 7.83 55.1 10/16/2013 6.68 54.1 1/13/2014 6.79 56.2 5/7/2014 7.57 52.1 8/6/2014 5.1 55 10/8/2014 5.75 57.6 2/18/2015 6.41 55.9 Piezometer 2 Date Nitrate (mg/1) Chloride (mg/1) 2/19/2009 0.5 NA 7/14/2009 0.5 7 9/22/2009 0.5 17 10/27/2009 0.6 7 6/2/2010 0.6 8 7/19/2010 0.6 8 12/10/2010 0.2 6 1/31/2011 0.3 9 4/25/2011 0.3 8 7/25/2011 0.1 9 10/19/2011 0.1 8 1/11/2012 0.1 9 4/20/2012 0.2 8 7/27/2012 0.2 9 10/17/2012 0.192 9.5 2/19/2013 0.218 9.67 4/24/2013 0.172 10.3 8/28/2013 0.198 9.66 10/16/2013 0.364 9.22 1/13/2014 0.169 11.4 5/7/2014 0.736 11.4 8/6/2014 0.8 12 10/8/2014 0.755 12.2 2/18/2015 0.749 12.6 Piezometer 3 Date Nitrate (mg/1) Chloride (mg/1) 2/19/2009 0.7 NA 7/14/2009 0.8 12 9/22/2009 0.8 24 10/27/2009 1.2 19 3/24/2010 1.7 116 6/2/2010 1.6 36 7/19/2010 1.6 35 12/10/2010 1.8 25 1/31/2011 1.8 40 4/25/2011 1.7 35 7/25/2011 1.8 61 10/19/2011 1.7 12 1/11/2012 1.8 20 4/20/2012 1.7 53 7/27/2012 1.8 21 10/17/2012 2.75 20.1 2/19/2013 1.85 21 4/24/2013 1.83 21.2 8/28/2013 1.81 22.4 10/16/2013 1.80 23.5 1/13/2014 1.70 26.0 5/7/2014 1.79 23.9 8/6/2014 1.7 26 10/8/2014 1.74 28.3 2/18/2015 1.82 27.1 TWN-1 Date Nitrate (mg/1) Chloride (mg/1) 2/6/2009 0.7 19 7/21/2009 0.4 17 9/21/2009 0.4 19 10/28/2009 0.5 18 3/17/2010 0.5 17 5/26/2010 0.6 20 9/27/2010 0.6 19 12/7/2010 0.6 14 1/26/2011 0.5 17 4/20/2011 0.5 19 7/26/2011 0.5 14 10/17/2011 0.5 10 1/9/2012 0.6 15 4/18/2012 0.6 17 7/24/2012 0.6 17 10/15/2012 0.432 17.5 2/18/2013 0.681 17.6 4/23/2013 0.84 17.4 8/27/2013 1.24 24.1 10/16/2013 1.61 26.8 1/14/2014 1.47 29.2 5/6/2014 1.63 31.1 8/5/2014 1.7 28 10/8/2014 1.46 27.6 2/18/2015 1.37 27.8 TWN-2 Date Nitrate (mg/1) Chloride (mg/1) 2/6/2009 25.4 29 7/21/2009 25 25 9/21/2009 22.6 17 11/2/2009 20.8 55 3/24/2010 62 .1 85 6/2/2010 69 97 9/29/2010 69 104 12/9/2010 48 93 2/1/2011 43 93 4/28/2011 40 85 7/28/2011 33 74 10/20/2011 33 76 1/12/2012 31 86 4/20/2012 48 103 7/31/2012 54 93 10/17/2012 22.1 79 2/19/2013 57.3 80.5 4/24/2013 57.7 82.1 8/27/2013 80 75.9 10/16/2013 111 70.4 1/13/2014 42.6 72.4 5/7/2014 44.7 84.9 8/6/2014 42 80 10/8/2014 70.6 81 2/18/2015 48.6 84.8 TWN-3 Date Nitrate (mg/1) Chloride (mg/1) 2/6/2009 23.6 96 7/21/2009 25.3 96 9/21/2009 27.1 99 11/2/2009 29 106 3/25/2010 25.3 111 6/3/2010 26 118 7/15/2010 27 106 12/10/2010 24 117 2/1/2011 24 138 4/28/2011 26 128 7/29/2011 25 134 10/20/2011 25 129 1/12/2012 25 143 4/20/2012 24 152 7/31/2012 27 158 10/17/2012 12.1 149 2/19/2013 22.2 157 4/24/2013 27.2 158 8/28/2013 20.9 171 10/17/2013 23.5 163 1/15/2014 19.6 160 5/7/2014 23.6 168 8/6/2014 19.5 174 10/9/2014 19.1 153 2/19/2015 19.4 164 TWN-4 Date Nitrate (mg/1) Chloride (mg/1) 2/6/2009 1 13 7/21/2009 0.05 12 9/21/2009 0.4 13 10/28/2009 0.4 11 3/16/2010 0.9 22 5/27/2010 1.0 22 9/27/2010 0.9 19 12/8/2010 1 21 1/25/2011 0.9 21 4/20/2011 0.9 21 7/26/2011 1.1 35 10/18/2011 0.9 20 1/9/2012 0.9 20 4/18/2012 1.1 24 7/25/2012 1.4 25 10/15/2012 1.45 26.4 2/18/2013 1.51 25.3 4/23/2013 1.63 24.4 8/27/2013 1.58 27.2 10/16/2013 1.69 29.4 1/14/2014 1.41 28.4 5/6/2014 1.55 29.6 8/5/2014 2.0 28 10/8/2014 1.44 30.7 2/18/2015 1.48 31.5 TWN-7 Date Nitrate (mg/1) Chloride (mg/1) 8/25/2009 ND 11.00 9/21/2009 ND 7.00 11/10/2009 0.1 7.00 3/17/2010 0.8 6.00 5/28/2010 1.2 6.00 7/14/2010 1.6 7.00 12/10/2010 1 4.00 1/27/2011 1.3 6.00 4/21/2011 1.7 6.00 7/29/2011 0.7 5.00 10/19/2011 2.2 6.00 1/11/2012 2.3 5.00 4/20/2012 1.2 6.00 7/26/2012 0.9 6.00 10/16/2012 0.641 5.67 2/19/2013 0.591 5.68 4/24/2013 1.16 5.88 8/28/2013 0.835 6.96 10/16/2013 0.986 5.70 1/15/2014 0.882 5.75 5/7/2014 0.564 5.26 8/6/2014 0.9 6.00 10/9/2014 0.968 5.93 2/19/2015 1.04 5.58 TWN-18 Date Nitrate (mg/1) Chloride (mg/1) 11/2/2009 1.3 57 3/17/2010 1.6 42 6/1/2010 1.8 63 9/27/2010 1.8 64 12/9/2010 1.6 59 1/27/2011 1.4 61 4/26/2011 1.8 67 7/28/2011 1.8 65 10/18/2011 1.9 60 1/10/2012 1.9 64 4/19/2012 2.1 64 7/26/2012 2.3 67 10/16/2012 1.95 67.5 2/18/2013 2.27 68.7 4/23/2013 2.32 64.3 8/27/2013 2.04 70.4 10/16/2013 2.15 67.3 1/14/2014 2.33 68.4 5/6/2014 2.18 76.5 8/5/2014 1.8 70 10/8/2014 1.47 74.8 2/18/2015 1.00 73.3 TW4-19 Date Nitrate (mg/1) Date Chloride (mg/1) 7/22/2002 42.80 12/7/2005 81 9/12/2002 47.60 3/9/2006 86 3/28/2003 61.40 7/20/2006 123 6/23/2003 11.40 11/9/2006 134 7/15/2003 6.80 2/28/2007 133 8/15/2003 4.00 8/15/2007 129 9/12/2003 5.70 10/10/2007 132 9/25/2003 9.20 3/26/2008 131 10/29/2003 7.70 6/25/2008 128 11/9/2003 4.80 9/10/2008 113 8/16/2004 9.91 10/15/2008 124 9/17/2004 4.50 3/4/2009 127 3/16/2005 5.30 6/23/2009 132 6/7/2005 5.70 9/14/2009 43 8/31/2005 4.60 12/14/2009 124 12/1/2005 0.10 2/17/2010 144 3/9/2006 4.00 6/9/2010 132 6/14/2006 5.20 8/16/2010 142 7/20/2006 4.30 10/11/2010 146 11/9/2006 4.60 2/17/2011 135 2/28/2007 4.00 6/7/2011 148 8/15/2007 4.10 8/17/2011 148 10/10/2007 4.00 11/17/2011 148 3/26/2008 2.20 1/23/2012 138 6/25/2008 2.81 6/6/2012 149 9/10/2008 36.20 9/5/2012 149 10/15/2008 47.80 10/3/2012 150 3/4/2009 3.20 2/11/2013 164 6/23/2009 2.40 6/5/2013 148 9/14/2009 0.10 9/3/2013 179 12/14/2009 26.70 10/29/2013 206 2/17/2010 2.00 1/27/2014 134 6/9/2010 4.40 5/19/2014 152 8/16/2010 5.90 8/11/2014 140 10/11/2010 2.70 10/21/2014 130 2/17/2011 17.00 3/9/2015 238 6/7/2011 12.00 8/17/2011 3.00 11/17/2011 5.00 1/23/2012 0.60 6/6/2012 2.40 9/5/2012 2.50 10/3/2012 4.10 2/11/2013 7.99 6/5/2013 2.95 9/3/2013 17.60 10/29/2013 4.70 1/27/2014 1.62 5/19/2014 1.34 8/11/2014 1.60 10/21/2014 4.72 3/9/2015 8.56 The sampling program for TW4-19 was updated in the fourth quarter of 2005 to include analysis for chloride as well as nitrate. This change accounts for the different number of data points represented above. TW4-21 Date Nitrate (mg/1) Date Chloride (mg/1) 5/25/2005 14.6 12/7/2005 353 8/31/2005 10.1 3/9/2006 347 11/30/2005 9.6 7/20/2006 357 3/9/2006 8.5 11/8/2006 296 6/14/2006 10.2 2/28/2007 306 7/20/2006 8.9 6/27/2007 327 11/8/2006 8.7 8/15/2007 300 2/28/2007 8.7 10/10/2007 288 6/27/2007 8.6 3/26/2008 331 8/15/2007 8.6 6/25/2008 271 10/10/2007 8.3 9/10/2008 244 3/26/2008 14.3 10/15/2008 284 6/25/2008 8.8 3/11/2009 279 9/10/2008 7.6 6/24/2009 291 10/15/2008 8.0 9/15/2009 281 3/11/2009 8.3 12/22/2009 256 6/24/2009 8.1 2/25/2010 228 9/15/2009 9.2 6/10/2010 266 12/22/2009 8.4 8/12/2010 278 2/25/2010 8.4 10/13/2010 210 6/10/2010 12.0 2/22/2011 303 8/12/2010 14.0 6/1/2011 297 10/13/2010 7.0 8/17/2011 287 2/22/2011 9.0 11/16/2011 276 6/1/2011 13.0 1/19/2012 228 8/17/2011 14.0 6/13/2012 285 11/16/2011 13.0 9/13/2012 142 1/19/2012 15.0 10/4/2012 270 6/13/2012 11.0 2/13/2013 221 9/13/2012 13.0 6/18/2013 243 10/4/2012 14.0 9/12/2013 207 2/13/2013 11.8 11/13/2013 206 6/18/2013 13.8 2/5/2014 200 9/12/2013 10.3 5/22/2014 243 11/13/2013 9.0 8/27/2014 230 2/5/2014 11.4 10/29/2014 252 5/22/2014 11.5 3/12/2015 255 8/27/2014 7.1 10/29/2014 10.0 3/12/2015 10.9 The sampling program for TW4-21 was updated in the fourth quarter of 2005 to include analysis for chloride as well as nitrate. This change accounts for the different number of data points represented above. TW4-22 Date Nitrate (mg/1) Chloride (mg/1) 2/28/2007 20.9 347 6/27/2007 19.3 273 8/15/2007 19.3 259 10/10/2007 18.8 238 3/26/2008 39.1 519 6/25/2008 41.9 271 9/10/2008 38.7 524 10/15/2008 36.3 539 3/11/2009 20.7 177 6/24/2009 20.6 177 9/15/2009 40.3 391 12/29/2009 17.8 175 3/3/2010 36.6 427 6/15/2010 19 134 8/12/2010 18 127 8/24/2010 15 130 10/13/2010 16 134 2/23/2011 18 114 6/1/2011 17 138 8/17/2011 15 120 11/16/2011 19 174 1/19/2012 14 36 6/13/2012 12.8 35 9/12/2012 7 121 10/4/2012 14 130 2/11/2013 58 635 6/5/2013 50.2 586 9/3/2013 29.7 487 10/29/2013 45.2 501 1/27/2014 54.6 598 5/19/2014 47.2 614 8/11/2014 41.5 540 10/21/2014 54.9 596 3/9/2015 69.2 675 TW4-24 Date Nitrate (mg/1) Chloride (mg/1) 6/27/2007 26.1 770 8/15/2007 29 791 10/10/2007 24.7 692 3/26/2008 24.4 740 6/25/2008 45.3 834 9/10/2008 38.4 1180 10/15/2008 44.6 1130 3/4/2009 30.5 1010 6/24/2009 30.4 759 9/15/2009 30.7 618 12/17/2009 28.3 1080 2/25/2010 33.1 896 6/9/2010 30 639 8/11/2010 32 556 8/24/2010 31 587 10/6/2010 31 522 2/17/2011 31 1100 5/26/2011 35 1110 8/17/2011 34 967 11/16/2011 35 608 1/18/2012 37 373 6/6/2012 37 355 8/30/2012 37 489 10/3/2012 38 405 2/11/2013 35.9 1260 6/5/2013 23.7 916 9/3/2013 32.6 998 10/29/2013 34.6 1030 1/27/2014 31.6 809 5/19/2014 35 1020 8/11/2014 31.5 1150 10/21/2014 35.7 1050 3/9/2015 34.6 944 TW4-25 Date Nitrate (mg/1) Chloride (mg/1) 6/27/2007 17.1 395 8/15/2007 16.7 382 10/10/2007 17 356 3/26/2008 18.7 374 6/25/2008 22.1 344 9/10/2008 18.8 333 10/15/2008 21.3 366 3/4/2009 15.3 332 6/24/2009 15.3 328 9/15/2009 3.3 328 12/16/2009 14.2 371 2/23/2010 14.4 296 6/8/2010 16 306 8/10/2010 14 250 10/5/2010 15 312 2/16/2011 15 315 5/25/2011 16 321 8/16/2011 16 276 11/15/2011 16 294 1/18/2012 16 304 5/31/2012 16 287 9/11/2012 17 334 10/3/2012 17 338 2/11/2013 9.04 190 6/5/2013 5.24 136 9/3/2013 5.69 119 10/29/2013 6.10 88.6 1/27/2014 2.16 85.7 5/19/2014 1.21 51.1 8/11/2014 1.6 67 10/21/2014 1.03 58.1 3/9/2015 14.4 310 MW-30 Date Nitrate (mg/1) Date Chloride (mg/1) 6/22/2005 12.4 6/22/2005 125 9/22/2005 12.8 9/22/2005 125 12/14/2005 13.6 12/14/2005 128 3/22/2006 13.8 3/22/2006 125 6/21/2006 14.5 6/21/2006 124 9/13/2006 14.1 9/13/2006 118 10/25/2006 14.6 10/25/2006 124 3/15/2007 14.4 3/15/2007 125 8/22/2007 14.6 8/22/2007 126 10/24/2007 14.9 10/24/2007 122 3/19/2008 14.8 3/19/2008 118 6/3/2008 18.7 6/3/2008 125 8/4/2008 17.3 8/4/2008 121 11/5/2008 15.6 11/5/2008 162 2/3/2009 15.3 2/3/2009 113 5/13/2009 15.1 5/13/2009 122 8/24/2009 20.9 8/24/2009 118 10/14/2009 15.0 10/14/2009 129 1/20/2010 15.4 1/20/2010 106 2/9/2010 16.1 2/9/2010 127 4/27/2010 15.8 4/27/2010 97 5/24/2010 17.0 9/14/2010 111 6/15/2010 15.3 11/9/2010 126 8/24/2010 16.0 2/1/2011 134 9/14/2010 15.0 4/11/2011 134 10/19/2010 15.0 5/10/2011 128 11/9/2010 15.0 6/20/2011 127 12/14/2010 16.0 7/5/2011 127 1/10/2011 15.0 8/3/2011 126 2/1/2011 16.0 9/7/2011 145 3/14/2011 17.0 10/4/2011 129 4/11/2011 16.0 11/8/2011 122 5/10/2011 16.0 12/12/2011 124 6/20/2011 17.0 1/24/2012 124 7/5/2011 17.0 2/14/2012 126 8/3/2011 14.0 3/14/2012 128 9/7/2011 16.0 4/10/2012 128 10/4/2011 16.0 5/2/2012 124 11/8/2011 16.0 6/18/2012 131 12/12/2011 16.0 7/10/2012 128 1/24/2012 17.0 8/7/2012 139 2/14/2012 17.0 9/19/2012 130 3/14/2012 18.0 10/23/2012 135 4/10/2012 17.0 11/13/2012 114 5/2/2012 16.0 12/26/2012 122 MW-30 Date Nitrate (mg/1) Date Chloride (mg/1) 6/18/2012 15.0 1/23/2013 128 7/10/2012 17.0 2/26/2013 129 8/7/2012 18.0 3/20/2013 126 9/19/2012 16.0 4/17/2013 117 10/23/2012 16.2 5/15/2013 119 11/13/2012 18.5 6/25/2013 127 12/26/2012 17.2 7/10/2013 130 1/23/2013 19.2 8/20/2013 126 2/26/2013 21.4 9/18/2013 131 3/20/2013 14.3 10/22/2013 128 4/17/2013 16.8 11/20/2013 124 5/15/2013 18.8 12/18/2013 134 6/25/2013 16.1 1/8/2014 131 7/10/2013 17.6 2/25/2014 135 8/20/2013 16.4 3/11/2014 144 9/18/2013 16.9 4/23/2014 154 10/22/2013 19.7 5/14/2014 128 11/20/2013 19.5 6/3/2014 128 12/18/2013 20.7 7/29/2014 140 1/8/2014 20.3 8/20/2014 139 2/25/2014 18.4 9/9/2014 136 3/11/2014 21.3 10/7/2014 136 4/23/2014 18.3 11/10/2014 154 5/14/2014 17.9 12/10/2014 138 6/3/2014 19.4 1/21/2015 144 7/29/2014 15.6 2/4/2015 136 8/20/2014 13.8 3/3/2015 132 9/9/2014 16.8 10/7/2014 11.0 11/10/2014 16.2 12/10/2014 17.1 1/21/2015 19.5 2/4/2015 14.9 3/3/2015 17.3 Under the groundwater sampling program, accelerated monitoring for nitrate began in MW- 30 prior to when the accelerated monitoring for chloride began. This difference accounts for the different number of data points represented above. MW-31 Date Nitrate (mg/1) Date Chloride (mg/1) 6/22/2005 24.2 6/22/2005 139 9/22/2005 22.4 9/22/2005 136 12/14/2005 23.8 12/14/2005 135 3/22/2006 24.1 3/22/2006 133 6/21/2006 25.3 6/21/2006 138 9/13/2006 24.6 9/13/2006 131 10/25/2006 25.1 10/25/2006 127 3/15/2007 23.2 3/15/2007 132 3/15/2007 22.0 3/15/2007 132 8/27/2007 23.3 8/27/2007 136 10/24/2007 24.6 10/24/2007 122 3/19/2008 25.0 3/19/2008 124 6/3/2008 29.3 6/3/2008 128 8/4/2008 28.7 8/4/2008 124 11/11/2008 29.9 11/11/2008 119 2/3/2009 23.4 2/3/2009 115 5/13/2009 22.4 5/13/2009 124 8/24/2009 15.4 8/24/2009 122 10/14/2009 22.6 10/14/2009 138 2/9/2010 21.7 2/9/2010 128 4/20/2010 22.5 4/20/2010 128 5/21/2010 23.0 9/13/2010 139 6/15/2010 21.1 11/9/2010 138 8/24/2010 22.0 2/1/2011 145 9/13/2010 21.0 4/1/2011 143 10/19/2010 20.0 5/10/2011 143 11/9/2010 20.0 6/20/2011 145 12/14/2010 20.0 7/5/2011 148 1/10/2011 19.0 8/2/2011 148 2/1/2011 21.0 9/6/2011 148 3/14/2011 22.0 10/3/2011 145 4/1/2011 21.0 11/8/2011 145 5/10/2011 20.0 12/12/2011 148 6/20/2011 22.0 1/24/2012 155 7/5/2011 22.0 2/13/2012 150 8/2/2011 20.0 3/13/2012 152 9/6/2011 21.0 4/9/2012 160 10/3/2011 21.0 5/2/2012 151 11/8/2011 21.0 6/18/2012 138 12/12/2011 21.0 7/9/2012 161 1/24/2012 21.0 8/6/2012 175 2/13/2012 21.0 9/18/2012 172 3/13/2012 22.0 10/22/2012 157 4/9/2012 21.0 11/6/2012 189 5/2/2012 20.0 12/18/2012 170 MW-31 Date Nitrate (mg/1) Date Chloride (mg/1) 6/18/2012 21.6 1/22/2013 176 7/9/2012 21.0 2/19/2013 174 8/6/2012 21.0 3/19/2013 168 9/18/2012 21.0 4/16/2013 171 10/22/2012 18.0 5/13/2013 169 11/6/2012 23.6 6/24/2013 179 12/18/2012 22.2 7/9/2013 182 1/22/2013 22.8 8/19/2013 183 2/19/2013 19.3 9/17/2013 193 3/19/2013 19.1 10/23/2013 188 4/16/2013 18.8 11/18/2013 174 5/13/2013 23.8 12/17/2013 203 6/24/2013 20.0 1/7/2014 194 7/9/2013 21.7 2/17/2014 197 8/19/2013 16.0 3/10/2014 230 9/17/2013 21.2 4/28/2014 230 10/23/2013 21.2 5/13/2014 200 11/18/2013 23.9 6/2/2014 173 12/17/2013 24.2 7/28/2014 200 1/7/2014 24.0 8/18/2014 210 2/17/2014 20.6 9/3/2014 210 3/10/2014 26.2 10/6/2014 205 4/28/2014 19.1 11/4/2014 204 5/13/2014 23.3 12/9/2014 215 6/2/2014 23.1 1/20/2015 226 7/28/2014 19.0 2/2/2015 211 8/18/2014 15.2 3/3/2015 209 9/3/2014 18.9 10/6/2014 15.9 11/4/2014 20.9 12/9/2014 17.0 1/20/2015 20.9 2/2/2015 18.7 3/3/2015 19.8 Under the groundwater sampling progran, accelerated monitoring for nitrate began in MW-31 prior to when the accelerated monitoring for chloride began . This difference accounts for the different number of data points represented above. TabK Concentration Trend Graphs (mg/L) 0 Feb-08 +----4~--~----+----;-----r----+---~-----r----~--_, 0 01 00 Jul-09 Nov-10 Apr-12 Aug-13 Dec-14 · May-16 ~--~~--~----~--~----~----~--~----~----~--~ ""C CD N 0 3 CD -CD ""' ...... z ;:::;: ""' Q) -CD (") 0 :::s () CD :::s -""' Q) :::::!'. 0 :::s en 0 0 1\) 0 w 0 (mg/L) 01 0 (j) 0 CXl 0 co 0 Feb-08 +-----~----~----~----~-----r-----+-----+-----+----~ Jul-09 - Nov-10 Apr-12 Aug-13 Dec-14 - May-16 -~----~----~----~----~----~----~----~----~----~ ""C (I) N 0 3 (I) -(I) ""' ...... 0 :::r 0 :::::!. a. (I) 0 0 ::::J (") (I) ::::J -""' D) :::::!'. 0 ::::J Ch 0 Feb-08 Jul-09 - Nov-10 Apr-12 Aug-13 Dec-14 - May-16 0 1\J 0 c.u ~< ~ ~ ,..---~~ ~ ~~ ~ ~ \ ~ ... ------- ~ ~ (mg/L) 0 01 ~ ~ ~ ~~ -~ ~ l..-----~ ........ ~ )~ ~~ 0 <0 ""C a;· N 0 3 ! C'D """ 1\) z ;::::;: """ a C'D 0 0 ::::s (') C'D ::::s -""" D) !:!'. 0 ::::s en 0 Feb-08 Jul-09 Nov-10 ' Apr-12 - Aug-13 - Dec-14 May-16 1\) (mg/L) ...... 0) CXl 0 1\) .... \ . . ~· ~ ~ ~ '~ I ~~ ~ \~ \ ...... ...... 0) CXl "'tJ CD N 0 3 a CD ""' !\) 0 :::r 0 ~. c. CD 0 0 ::I (') CD ::I -""' D) !:!'. 0 ::I en (mg/L) 0 Feb-08 +--------+--------r--------r------~--------+-------_, 0 (J1 1\) (J1 Jul-09 Nov-10 - Apr-12 Aug-13 Dec-14 May-16 ~------~--------~------~------~--------~------~ "'C a;· N 0 3 C1) -C1) "" w z ;::::;: "" D) -C1) (") 0 :::J (') (1) :::J -"" D) -()' :::J t/1 0 Feb-08 Jul-09 Nov-10 Apr-12 - Aug-13 Dec-14 May-16 1\) 0 ' ~ .. .j:>. 0 ~ (J) 0 ~ ~ ~ ~ ~ > ~ ~~ \ ~ ~~ ~ (mg/L) (X) 0 ...... 0 0 ' 1\) 0 "tt (I) N 0 3 a (I) ""t (,) 0 '::r 0 :::::!. a. (I) 0 0 ::::s () (I) ::::s -""t D) e. 0 ::::s C/1 0 Feb-08 Jul-09 - Nov-10 Apr-12 Aug-13 Dec-14 May-16 0 <:n ~/ / ~~~· "' ~ ~ ~ . ~ \~ ~~ ~ (mg/L) 0 (X) < ~ ~ ~ ~ -( r ~ !r D. ~ z I ...... (mg/L) ...... ...... 0 1\) 0 1\) 01 (.0 0 (.0 01 01 01 0 Feb-08 +-------~----~-------+------~------+-------~----~ Jul-09 - Nov-10 - Apr-12 Aug-13 - Dec-14 , ~ z I ...A. (") ::::r 0 ""' a: (I) (") 0 ::::J (') (I) ::::J -""' ~ -s· ::::J Ch (mg/L) 1\) 0 0) 0 0 Feb-08 -r--------r--------~------~------_,--------+--------1 ()) 0 0 0 1\) 0 Jul-09 - Nov-10 Apr-12 Aug-13 Dec-14 May-16 ~------~------~------~~------~------~------~ ---4 :e z I N z :::::;: ""'' D) -(I) (") 0 ::::J (") (I) ::::J -""'' D) -s· ::::J t/1 (mg/L) 1\) 0 0> 0 CX> 0 0 0 0 Feb-08 +--------+--------r--------r------~~------;-------~ 1\) 0 Jul-09 Nov-10 Apr-12 Aug-13 Dec-14 --4 ::e z I N 0 :::r 0 .., 0: CD 0 0 ::::s (') CD ::::s -.., D) -c;· ::::s en (mg/L) 0 1\) 01 w 0 01 0 Feb-08 +-------r-----_,-------+------~------+-------~-----4 01 w 01 Jul-09 - Nov-10 Apr-12 Aug-13 · Dec-14 May-16 ~------~----~------~------~------~----~------~ -1 ::E z I w z ;::j.' """ Q) ..... (1) 0 0 ::::::1 n (1) ::::::1 ..... """ Q) ..... (5' ::::::1 en 0 Feb-08 Jul-09 - Nov-10 . Apr-12 Aug-13 ' Dec-14 May-16 1\) 0 0> 0 (X) 0 (mg/L) ~ ~ 0 0 ~ 1\) 0 ...... 0> 0 !,> ~ ~ ). ~ ...... (X) 0 1\) 0 0 --4 ::e z I (.,) (') ':r 0 :::::!. a. C'D (') 0 ::::s n C'D ::::s r+ ""' D) r+ cs· ::::s en 0 9 01 (mg/L) 1\) 1\) 01 Feb-08 +----------r--------~----------~--------,_ ________ _, Jul-09 Nov-10 Apr-12 Aug-13 - Dec-14 May-16 ~--------~--------~----------~--------~--------~ ~ z I ol:lo z ::::. ""' I» -(I) 0 0 :::1 " (I) :::1 -""' I» e. 0 :::1 (/1 0 0'1 0 (mg/L) 1\) 0 1\) 0'1 c.u 0'1 Feb-08 +-----~-----4------+-----~----~------+-----~-----4 Jul-09 • Nov-10 - Apr-12 Aug-13 - Dec-14 May-16 ~-----L----~------~----~----~------~----~-----4 -4 =E z I ~ 0 ::::r 0 '"'I c: CD 0 0 :::J (") CD :::J -'"'I D) -c;· :::J "' (mg/L) 0 1\) 1\) 01 Jul-09 +------+------1------1--------+--------: Nov-10 Apr-12 Aug-13 Dec-14 -f :E z I """" z ;:::;: ""''I D) -(I) (") 0 ~ (') (I) ~ -""''I D) !:!'. 0 ~ t/1 0 0 0 1\) 0 0 .j:>. 0 0 <rootL) 0 0 00 0 0 0 0 0 ...... 1\) 0 0 Feb-08 +--------+--------~-------r------_,--------+-------~ Jul-09 Nov-10 Apr-12 · Aug-13 - Dec-14 May-16 ~------~------~~------~------~--------~------~ -1 :e z I """"' (") :::r 0 ~-a. CD (") 0 ::::J (") CD ::::J -., Q) :::t. 0 ::::J C/1 p 0 c..n (mg/L) 1\:) c..n Jul-09 -t---------1------+-------if-------+--------l Nov-10 Apr-12 Aug-13 Dec-14 May-16 ~----~----~-----._ _____ ~--------~ -4 :e z I .... ()C) z :::;: ""'' D) -(I) 0 0 :::::5 (') (I) :::::5 -""'' D) -(5" :::::5 Ul 0 0 1\) 0 w 0 (mg/L) (11 0 0) 0 CXl 0 c.o 0 Jul-09 +---+---+---+---+----"1-----1----+---+----l Nov-10- Apr-12 Aug-13 - Dec-14 - May-16 ~--~--~--~-~~---"--~--~--~--~ ~ z I ...... co (") :::r 0 ~. c. CD (") 0 ::::s (') CD ::::s r+ "" ! (5' ::::s Ul 0 0 0 7/1/2002 11/1/2002 3/1/2003 7/1/2003 - 11/1/2003 3/1/2004 7/1/2004 11/1/2004 3/1/2005 7/1/2005 11/1/2005 - 3/1/2006 - 7/1/2006 11/1/2006 3/1/2007 7/1/2007 11/1/2007 3/1/2008 7/1/2008 11/1/2008 . 3/1/2009 7/1/2009 11/1/2009 3/1/2010 7/1/2010 11/1/2010 3/1/2011 7/1/2011 11/1/2011 3/1/2012 7/1/2012 11/1/2012 3/1/2013 7/1/2013 11/1/2013 3/1/2014 7/1/2014 11/1/2014 3/1/2015 - ...... 0 0 0 N 0 0 0 w 0 0 0 ~ 0 0 VI 0 0 0 "' 0 0 0 -...J 0 0 0 -· r+ ... QJ r+ tD n 0 ::::::s n tD ::::::s r+ ... 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CD n 0 ::::J n CD ::::J r+ .., QJ r+ -· 0 ::::J "' TabL CSV Transmittal Letter Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Kathy Weinel Wednesday, May 20, 2015 7:33AM Rusty Lundberg (rlundberg@utah.gov) 'Phil Goble'; 'Dean Henderson'; Harold Roberts; David Frydenlund; Scott Bakken; David Turk; Jaime Massey; Dan Hillsten; Logan Shumway Transmittal of CSV Files White Mesa Mill 2015 Q1 Nitrate Monitoring 1502347-EDD.csv Attached to this e-mail is an electronic copy of laboratory results for nitrate monitoring conducted at the White Mesa Mill during the first quarter of 2015, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel Jl,£ Energy Fuels Resources (USA) Inc. Kathy Weinel Quality Assurance Manager t: 303.389.4134 1 t: 303.389.4125 225 Union Blvd., Suite 600 Lakewood, CO 80228 http://www.energvtuels.com This e-mail is intended for the exclusive use of person(s) mentioned as the recipient(s). This message and any attached files with it are confidential and may contain privileged or proprietary information. If you are not the intended recipient(s) please delete this message and notify the sender. You may not use, distribute print or copy this message if you are not the intended recipient(s). 1 Tab M Residual Mass Estimate Analysis Figures and Tables Tab M -Figures Tab M -Tables g $ Ill E ·;; w Ill Ill Ill :5 Gl E :::J ii: ~ -z 45000~------------------------------------------------------------------------------------------------~ 40000 1 ....._....... , \ / \ 7 \ I ,__ / I \ L \ --.... ....._ 350001 \7 --- -------- 30000 T-----------------------------------------------------------------~~------------~------------------~ 25000 1-----------------------------------------------------------------------~Jf----------------------l y = -1043.5x + 41394 20000 +.--------~---------r---------r--------~--------~--------~--------~--------r---------~------~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ / ~ ~ ~ ~ ~ ~ ~ ~ ~ -N~rate Plume Mass Estimates HYDRO GEO CHEM,INC. Time Series of Nitrate Plume Mass Estimates --Linear (Nitrate Plume Mass Estimates) Approved ,Fjguro M.1 H:\718000\may15\nitrate\masscalc\Nmtrend0315: Bx11 LS Color