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HomeMy WebLinkAboutDRC-2015-001482 - 0901a06880507c5bFebruary 25, 2015 Sent VIA OVERNIGHT DELIVERY Mr. Rusty Lundberg Division of Radiation Control Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144850 Salt Lake City, UT 84114-4820 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www.cncrgyfuels.com DRC-2015-001482 Re: Transmittal of 4th Quarter 2014 Nitrate Monitoring Report Stipulation and Consent Order Docket Number UGW12-04 White Mesa Uranium Mill Dear Mr. Lundberg: Enclosed are two copies of the White Mesa Uranium Mill Nitrate Monitoring Report for the 4111 Quarter of 2014 as required by the Stipulation and Consent Order Docket Number UGW12-04, as well as two COs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours very truly, ci(mz;di~( ENERGY FUELS RESOURCES (USA) INC. Kathy Weinel Quality Assurance Manager cc: David C. Frydenlund Dan Hillsten Harold R. Roberts David E. Turk Scott Bakken White Mesa Uranium Mill Nitrate Monitoring Report State of Utah Stipulated Consent Agreement, January 2009 Docket No. UGW09-03 4th Quarter (October through December) 2014 Prepared by: Energy Fuels Resources (USA) Inc. 225 Union Boulevard, Suite 600 Lakewood, CO 80228 February 25, 2015 TABLE OF CONTENTS 1.0 INTRODUCTION ................................. , .............. a, •••••••••• " •••••••• " ................................ 1 2.0 GROUNDWATER NITRATE MONITORING ................................................ 1 2.1 Samples and Measurements Taken During the Quarter ..................................... 1 2.1.1 Nitrate Monitoring ...................................................................................... 2 2.1.2 Parameters Analyzed .................................................................................. 3 2.1.3 Groundwater Head and Level Monitoring ................................................... 3 2.2 Sampling Methodology and Equipment and Decontamination Procedures ....... 3 2.2.1 Well Purging, Sampling and Depth to Groundwater ................................... 4 2.2.2 Piezometer Sampling .................................................................................. 5 2.3 Field Data ............................................................................................................ 5 2.4 Depth to Groundwater Data and Water Table Contour Map .............................. 5 2.5 Laboratory Results .............................................................................................. 5 2. 5.1 Copy of Laboratory Results ... ;· ............. ., .................... · ........ · ............... ; .......... 5 2.5.2 Regulatory Framework ............................................................................... 5 3.0 QUALITY ASSURANCE AND DATA VALIDATION .................... n ............. 6 3.1 Field QC Samples ............................................................................................... 6 3.2 Adherence to Mill Sampling SOPs ..................................................................... 6 3.3 Analyte Completeness Review ........................................................................... 7 3.4 Data Validation ............................... , ................................ , ................................... 7 3.4.1 Field Data QA/QC Evaluation .................................................................... 7 3.4.2 Holding Time Evaluation ............................................................................. 8 3.4.3 Analytical Method Checklist ...................................................................... 8 3.4.4 Reporting Limit Evaluation ........................................................................ 8 3.4.5 QA/QC Evaluation for Sample Duplicates ............... , ................................. 9 3.4.6 Other Laboratory QA/QC ........................................................................... 9 3.4.7 Receipt Temperature Evaluation ................................................................. 10 3.4.8 Rinsate Check ........................................................................................... 10 4.0 INTERPRETATION OF DATA ....................................................................... 10 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions ........... 10 4.1.1 Current Site Groundwater Contour Map ................................................... 10 4.1.2 Comparison of Current Groundwater Contour Map to Groundwater Contour Map for Previous Quarter .................................................................................. 14 4.1.3 Hydrographs .............................................................................................. 15 4.1.4 Depth to Groundwater Measured and Groundwater Elevation ................. 15 4.2 Effectiveness of Hydraulic Containment and Capture ...................................... 15 4.2.1 Hydraulic Containment and Control.. ....................................................... 15 4.2.2 Current Nitrate and Chloride Isoconcentration Maps ............................... 18 4.2.3 Comparison of Areal Extent ............................................................................ 18 4.2.4 Nitrate and Chloride Concentration Trend Data and Graphs .................... 19 4.2.5 Interpretation of Analytical Data .............................................................. 19 4.3 Estimation of Pumped Nitrate Mass and Residual Nitrate Mass within the Plume .......................................................................................................................... 21 5.0 LONG TERM PUMP TEST AT TWN-02, TW4-22, TW4-24, and TW4-25 OPERATIONS REPORT .................................................................................. 24 5.1 Introduction .......................................................................................................... 24 1 5.2 Pumping Well Data Collection ......................................................................... 25 5.3 Water Level Measurements ............... -............................ -................................... 25 5.4 Pumping Rates and Volumes ............................................................................ 25 5.4.1 MW-04 ............................................................................................................. 26 5.4.2 TW4-04 ............................................................................................................ 27 5.4.3 MW-26 ............................................................................................................. 27 5.4.4 TW4-25 ........................................ -.................... -............. , .................................. 27 6.0 6.1 7.0 8.0 9.0 Table 1 Table 2 Table 3 Table 4 Table 5 Table 6 Table 7 Table 8 CORRECTIVE ACTION REPORT ................................................................. 28 Assessment of Previous Quarter's Corrective Actions ..................................... 28 CONCLUSIONS AND RECOMMENDATIONS ............................................ 28 ELECTRONIC DATA FILES AND FORMAT .............................................. 32 SIGNATURE AND CERTIFICATION ........................................................... 33 LIST OF TABLES Summary of Well Sampling and Constituents for the Period Nitrate Mass Removal Per Well Per Quarter Nitrate Well Pumping Rates and Volumes Quarterly Calculation of Nitrate mass Removed and Total Volume of Water Pumped Nitrate Data Over Time for MW-30, MW-31, MW-5, and MW-11 Slug Test Results Pre-Pumping Saturated Thickness Pre-Pumping Hydraulic Gradients and Flow Calculations 11 INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and Field Data Worksheets Tab C Kriged Current Quarter Groundwater Contour Map and Weekly, Monthly and Quarterly Depth to Water Data Tab D Kriged Previous Quarter Groundwater Contour Map Tab E Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells Tab F Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Tab G Laboratory Analytical Reports Tab H Quality Assurance and Data Validation Tables H-1 Field Data QA/QC Evaluation H-2 Holding Time Evaluation H-3 Analytical Method Check H-4 Reporting Limit Evaluation H-5 QA/QC Evaluation for Sample Duplicates H-6 QC Control limits for Analysis and Blanks H-7 Receipt Temperature Evaluation H-8 Rinsate Evaluation Tab I Kriged Current Quarter Nitrate and Chloride Isoconcentration Maps Tab J Analyte Concentration Data Over Time Tab K Nitrate and Chloride Concentration Trend Graphs Tab L CSV Transmittal Letter Tab M Residual Mass Estimate Analysis Figures and Tables 111 AWAL CA CAP CIR DIFB DRC EFRI ft amsl GWDP LCS MS MSD QA QAP QC RPD sco SOPs UDEQ voc ACRONYM LIST American West Analytical Laboratory Consent Agreement Corrective Action Plan Contamination Investigation Report Deionized Field Blanks Utah Division of Radiation Control Energy Fuels Resources (USA) Inc. feet above mean sea level Groundwater Discharge Permit Laboratory Control Spike Matrix Spike Matrix Spike Duplicate Quality Assurance Groundwater Monitoring Quality Assurance Plan Quality Control Relative Percent Difference Stipulated Consent Order Standard Operating Procedures Utah Department of Environmental Quality Volatile Organic Compounds iv 1.0 INTRODUCTION The Utah Department of Environmental Quality ("UDEQ") Division of Radiation Control ("DRC") noted in a Request dated September 30, 2008 (the "Request"), for a Voluntary Plan and Schedule to Investigate and Remediate Nitrate Contamination at the White Mesa Uranium Mill (the "Mill") (the "Plan"), that nitrate levels have exceeded the State water quality standard of 10 mg/L in certain monitoring wells. As a result of the Request, Energy Fuels Resources (USA) Inc. ("EFRI") entered into a Stipulated Consent Agreement with the Utah Water Quality Board in January 2009 which directed the preparation of a Nitrate Contamination Investigation Report ("CIR"). A subsequent letter dated December 1, 2009, among other things, recommended that EFRI also address elevated chloride concentrations in the CIR. The Stipulated Consent Agreement was amended in August 2011. Under the amended Consent Agreement ("CA"), EFRI submitted a Corrective Action Plan ("CAP"), pursuant to the requirements of the Utah Groundwater Quality Protection Rules [UAC R317-6-6.15(C -E)] on November 29, 2011 and revised versions of the CAP on February 27, 2012 and May 7, 2012. On December 12, 2012, DRC signed the Stipulation and Consent Order ("SCO"), Docket Number UGW12-04, which approved the EFRI CAP, dated May 7, 2012. The SCO ordered EFRI to fully implement all elements of the May 7, 2012 CAP. Based on the schedule included in the CAP and as delineated and approved by the SCO, the activities associated with the implementation of the CAP began in January 2013. The reporting requirements specified in the CAP and SCO are included in this quarterly nitrate report. This is the Quarterly Nitrate Monitoring Report, as required under the SCO, State of UDEQ Docket No. UGW12-04 for the fourth quarter of 2014. This report meets the requirements of the SCO, State of UDEQ Docket No. UGW12-04 and is the document which covers nitrate corrective action and monitoring activities during the fourth quarter of 2014. 2.0 GROUNDWATER NITRATE MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of all groundwater monitoring wells, piezometers, existing wells, temporary chloroform contaminant investigation wells and temporary nitrate investigation wells is attached under Tab A. Nitrate samples and measurements taken during this reporting period are discussed in the remainder of this section. 1 2.1.1 Nitrate Monitoring Quarterly sampling for nitrate monitoring parameters was performed in the following wells: TWN-1 TWN-2 TWN-3 TWN-4 TWN-7 TWN-18 TW4-22* TW4-24* TW4-25* Piezometer 1 Piezometer 2 Piezometer 3 As discussed in Section 2.1.2 the analytical constituents required by the CAP are inorganic chloride and nitrate+nitrite as N (referred to as nitrate in this document) * Wells TW4-22, TW4-24, TW4-25 are chloroform investigation wells (wells installed and sampled primarily for the chloroform investigation) and are sampled as part of the chloroform program. The analytical suite for these three wells includes nitrate, chloride and a select list of Volatile Organic Compounds ("VOCs") as specified in the chloroform program. These three wells are included here because they are being pumped as part of the remediation of the nitrate contamination as required by the SCO and the CAP. The nitrate and chloride data are included in this report as well as in the chloroform program quarterly report. The VOC data for these three wells will be repmted in the chloroform quarterly monitoring report only. The December 12, 2012 SCO approved the CAP, which specified the cessation of sampling in TWN-5, TWN-6, TWN-8, TWN-9, TWN-10, TWN-11, TWN-12, TWN-13, TWN-14, TWN-15, TWN-16, TWN-17, and TWN-19. The CAP and SCO also approved the abandonment ofTWN- 5, TWN-8, TWN-9, TWN-10, TWN-11, TWN-12, TWN-13, TWN-15, and TWN-17 within 1 year of the SCO approval. These wells were abandoned in accordance with the DRC-approved Well Abandonment Procedure on July 31, 2013 . Wells TWN-6, TWN-14, TWN-16, and TWN- 19 have been maintained for depth to groundwater monitoring only, as noted in the CAP. Table 1 provides an overview of all locations sampled during the current period, along with the date samples were collected from each location, and the date(s) upon which analytical data were received from the contract laboratory. Table 1 also identifies rinsate samples collected, as well as sample numbers associated with any required duplicates. As indicated in Table 1, nitrate monitoring was performed in the nitrate monitoring wells, chloroform wells TW4-22, TW4-24, TW4-25 and Piezometers 1, 2, and 3. Analytical data for all of the above-listed wells, and the piezometers, are included in Tab G. Nitrate and chloride are also monitored in all of the Mill's groundwater monitoring wells and chloroform investigation wells. Data from those wells for this quarter are incorporated in certain maps and figures in this report but are discussed in their respective programmatic reports. 2 2.1.2 Parameters Analyzed Locations sampled during this reporting period were analyzed for the following constituents: • Inorganic Chloride • Nitrate plus Nitrite as Nitrogen (referred to herein as nitrate) Use of analytical methods consistent with the requirements found in the White Mesa Mill Groundwater Quality Assurance Plan, ("QAP") Revision 7.2, dated June 6, 2012 was confirmed for all analytes, as discussed later in this report. 2.1.3 Groundwater Head and Level Monitoring Depth to groundwater was measured in the following wells and/or piezometers, pursuant to Part I.E.3 of the Groundwater Discharge Permit ("GWDP") (dated August 24, 2012): • The quarterly groundwater compliance monitoring wells • Existing well MW -4 and all of the temporary chloroform investigation wells • Piezometers-P-1, P-2, P-3, P-4 and P-5 • MW-20, MW-22, and MW-34 • The DR piezometers that were installed during the Southwest Hydrogeologic Investigation • Nitrate wells TWN-1, TWN-2, TWN-3, TWN-4, TWN-6, TWN-7, TWN-14, TWN-16, TWN-18 and TWN-19 In addition to the above, depth to water measurements are routinely observed in conjunction with sampling events for all wells sampled during quarterly and accelerated efforts, regardless of the sampling purpose. All well levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab C. Field data sheets for groundwater measurements are also provided in Tab C. Weekly and monthly depth to groundwater measurements were taken in the chloroform pumping wells MW-4, MW-26, TW4-19, TW4-20, and TW4-4, and the nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2. In addition, monthly water level measurements were taken in non-pumping wells MW-27, MW-30, MW-31, TW4-21, TWN-1, TWN-3, TWN-4, TWN-7, and TWN-18 as required by the CAP. 2.2 Sampling Methodology and Equipment and Decontamination Procedures The QAP provides a detailed presentation of procedures utilized for groundwater sampling activities under the GWDP (August 24, 2012). The sampling methodology, equipment and decontamination procedures that were performed for the nitrate contaminant investigation, as summarized below, are consistent with the QAP. 3 2.2.1 Well Purging, Sampling and Depth to Groundwater A list of the wells in order of increasing nitrate contamination is generated quarterly. The order for purging is thus established. The list is included with the Field Data Worksheets under Tab B. Mill personnel start purging with all of the nondetect wells and then move to the wells with detectable nitrate concentrations, progressing from the wells having the lowest nitrate contamination to wells with the highest nitrate contamination. Before leaving the Mill office, the pump and hose are decontaminated using the cleaning agents described in Attachment 2-2 of the QAP. Rinsate blanks are collected at a frequency of one rinsate per 20 field samples. Purging is completed to remove stagnant water from the casing and to assure that representative samples of formation water are collected for analysis. There are three purging strategies specified in the QAP that are used to remove stagnant water from the casing during groundwater sampling at the Mill. The three strategies are as follows: 1. Purging three well casing volumes with a single measurement of field parameters 2. Purging two casing volumes with stable field parameters (within 10% Relative Percent Difference ["RPD"]) 3. Purging a well to dryness and stability (within 10% RPD) of a limited list of field parameters after recovery. Mill personnel proceed to the first well, which is the well with the lowest concentration (i.e. non- dectect) of nitrate based on the previous quarter's sampling results. Well depth measurements are taken and the one casing volume is calculated. The purging strategy that will be used for the well is determined at this time based on the depth to water measurement and the previous production of the well. The Grundfos pump (a 6 to 10 gallon per minute [gpm] pump) is then lowered to the appropriate depth in the well and purging is started. At the first well, the purge rate is measured for the purging event by using a calibrated 5 gallon bucket. After the evacuation of the well has been completed, the well is sampled when possible, and the pump is removed from the well and the process is repeated at each well location moving from the least contaminated to most contaminated well. If sample collection is not possible due to the well being purged dry, a sample is collected after recovery using a disposable bailer and as described in Attachment 2-3 of the QAP. Sample collection follows the procedures described in Attachment 2-4 of the QAP. After the samples have been collected for a particular well, the samples are placed into a cooler that contains ice. The well is then recapped and Mill personnel proceed to the next well. If a bailer has been used it is disposed of. Decontamination of non-dedicated equipment, using the reagents in Attachment 2-2 of the QAP, is performed between each sample location, and at the beginning of each sampling day, in addition to the pre-event decontamination described above. 4 2.2.2 Piezometer Sampling Samples are collected from Piezometers 1, 2 and 3, if possible. Samples are collected from piezometers using a disposable bailer after one set of field measurements have been collected. Due to the difficulty in obtaining samples from the piezometers, the purging protocols set out in the QAP are not followed. After samples are collected, the bailer is disposed of and samples are placed into a cooler containing ice for sample preservation and transit to the Mill's contract analytical laboratory, American West Analytical Laboratories ("AW AL"). 2.3 Field Data Attached under Tab B are copies of all Field Data Worksheets that were completed during the quarter for the nitrate investigation monitoring wells and piezometers identified in Section 2.1.1 and Table 1. 2.4 Depth to Groundwater Data and Water Table Contour Map Depth-to-groundwater measurements that were utilized for groundwater contours are included on the Quarterly Depth to Water Sheet at Tab C of this Report along with the kriged groundwater contour map for the current quarter generated from this data. All well levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab C. A copy of the kriged groundwater contour map generated from the previous quarter's data is provided under Tab D. 2.5 Laboratory Results 2.5.1 Copy of Laboratory Results The analytical results were provided by AW AL. Table 1 lists the dates when analytical results were reported to the Quality Assurance ("QA") Manager for each well or other sample. Analytical results for the samples collected for this quarter's nitrate investigation and a limited list of chloroform investigation nitrate and chloride results are provided under Tab G of this Report. Also included under Tab G are the results of analyses for duplicate samples and rinsate samples for this sampling effort, as identified in Table 1. See the Groundwater Monitoring Report and Chloroform Monitoring Report for this quarter for nitrate and chloroform analytical results for the groundwater monitoring wells and chloroform investigation wells not listed in Table 1. 2.5.2 Regulatory Framework As discussed in Section 1.0 above, the Request, Plan, and CA each triggered a series of actions on EFRI's part. Potential surficial sources of nitrate and chloride have been described in the December 30, 2009 CIR and additional investigations into potential sources were completed and discussed with DRC in 2011. Pursuant to theCA, the CAP was submitted to the Director of the Division of Radiation Control (the "Director") on May 7, 2012. The CAP describes activities 5 associated with the nitrate in groundwater. The CAP was approved by the Director on December 12, 2012. This quarterly report documents the monitoring consistent with the program described in the CAP. 3.0 QUALITY ASSURANCE AND DATA VALIDATION EFRI's QA Manager performed a QA/Quality Control ("QC") review to confirm compliance of the monitoring program with the requirements of the QAP. As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and QC review of laboratory data methods and data. Identification of field QC samples collected and analyzed is provided in Section 3.1. Discussion of adherence to Mill sampling Standard Operating Procedures ("SOPs") is provided in Section 3.2. Analytical completeness review results are provided in Section 3.3. The steps and tests applied to check field data QA/QC, holding times, receipt temperature and laboratory data QA/QC are discussed in Sections 3.4.1 through 3.4.7 below. The analytical laboratory has provided summary reports of the analytical QA/QC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference certification and reporting protocol. The Analytical Laboratory QA/QC Summary Reports, including copies of the Mill's Chain of Custody and Analytical Request Record forms for each set of Analytical Results, follow the analytical results under Tab G. Results of the review of the laboratory QA/QC information are provided under Tab H and discussed in Section 3.4, below. 3.1 Field QC Samples The following QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program. Field QC samples for the nitrate investigation program consist of one field duplicate sample for each 20 samples, DI Field Blanks ("DIFB"), and equipment rinsate samples. During the quarter, one duplicate sample was collected as indicated in Table 1. The duplicate was sent blind to the analytical laboratory and analyzed for the same parameters as the nitrate wells. One rinsate blank sample was collected as indicated on Table 1. Rinsate samples are labeled with the name of the subsequently purged well with a terminal letter "R" added (e.g. TWN-7R). The field QC sample results are included with the routine analyses under Tab G. 3.2 Adherence to Mill Sampling SOPs The QA Manager review of Mill Personnel's adherence to the existing SOPs, confirmed that the QAJQC requirements established in the QAP and Chloroform QAP were met. 6 3.3 Analyte Completeness Review All analyses required by the GWDP for nitrate monitoring for the period were performed. 3.4 Data Validation The QAP and GWDP (August 24, 2012) identify the data validation steps and data QC checks required for the nitrate monitoring program. Consistent with these requirements, the QA Manager performed the following evaluations: a field data QA/QC evaluation, a holding time evaluation, an analytical method check, a reporting limit evaluation, a QC evaluation of sample duplicates, a QC evaluation of control limits for analysis and blanks, a receipt temperature evaluation, and a rinsate evaluation. Because no VOCs are analyzed for the nitrate contamination investigation, no trip blanks are required in the sampling program. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab H. 3.4.1 Field Data QA/QC Evaluation The QA Manager performs a review of all field recorded parameters to assess their adherence with QAP requirements. The assessment involved review of two sources of information: the Field Data Sheets and the Quarterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and stability of five parameters: conductance, pH, temperature, redox potential, and turbidity. Review of the Depth to Water data confirms that all depth measurements used for development of groundwater contour maps were conducted within a five-day period of each other. The results of this quarter's review are provided under Tab H. Based upon the review of the field data sheets, field work conformed with the QAP purging and field measurement requirements. A summary of the purging techniques employed and field measurements taken is described below: Purcing Two Casin~Z: Volumes with Stable Field Parameters (within 10% RPD) Wells TWN-01, TWN-04, and TWN-18 were sampled after two casing volumes were removed. Field parameters pH, specific conductivity, turbidity, water temperature, and redox potential were measured during purging. All field parameters for this requirement were stable within 10% RPD. Pmging a W 11 to Dryness aod Stability of a Lim.jtcd Li t of Field Parameter. Wells TWN-03 and TWN-07 were purged to dryness before two casing volumes were evacuated. After well recovery, one set of measurements for the field parameters of pH, specific conductivity, and water temperature only were taken; the samples were collected, and another set of measurements for pH, specific conductivity, and water temperature were taken. Stabilization of pH, conductivity and temperature are required within 10% RPD under the QAP. All field parameters for this requirement were stable within 10% RPD. Continuously Pumped Wells Wells TWN-02, TW4-22, TW4-24, and TW4-25 are continuously pumped wells. These wells are pumped on a set schedule per the remediation plan and are considered sufficiently evacuated to 7 immediately collect a sample. As previously noted, TW4-22, TW4-24, and TW4-25 are chloroform investigation wells and are sampled under the chloroform program. Data for nitrate and chloride are provided here for completeness purposes. During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water to the nearest 0.01 foot. All field parameters for all wells were within the QAP required limits, as indicated below. The review of the field sheets for compliance with QAP requirements resulted in the observations noted below. The QAP requirements in Attachment 2-3 specifically state that field parameters must be stabilized to within 10% over at least 2 consecutive measurements for wells purged to two casing volumes or to dryness. The QAP Attachment 2-3 states that turbidity should be less than 5 NTU prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP Attachment 2-3 does not require that turbidity measurements be less than 5 NTU prior to sampling. As such the noted observations regarding turbidity measurements greater than 5 NTU below are included for information purposes only. • Six well measurements exceeded the QAP's 5 NTU turbidity goal as noted in Tab H. All required turbidity RPD's met the QAP Requirement to stabilize within 10%. EFRI's letter to DRC of March 26, 2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In response to DRC's subsequent correspondence dated June 1, 2010 and June 24, 2010, EFRI completed a monitoring well redevelopment program. The redevelopment report was submitted to DRC on September 30, 2011. DRC responded to the redevelopment report via letter on November 15, 2012. Per the DRC letter dated November 15, 2012, the field data generated this quarter are compliant with the turbidity requirements of the approved QAP. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided in Tab H. All samples were received and analyzed within the required holding time. 3.4.3 Analytical Method Checklist All analytical methods reported by the laboratory were checked against the required methods enumerated in the QAP. Analytical method checks are provided in Tab H. All methods were consistent with the requirements of the QAP. 3.4.4 Reporting Limit Evaluation All analytical method reporting limits ("RLs") reported by the laboratory were checked against the reporting limits enumerated in the QAP. Reporting Limit Checks are provided in Tab H. All analytes were measured and reported to the required reporting limits, with the exception of several samples that had increased reporting limits due to matrix interference or required dilution due to the sample concentration. However, in all of those cases the analytical results were 8 greater than the reporting limit used. 3.4.5 QA/QC Evaluation for Sample Duplicates Section 9 .1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results are less than 5 times the required detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05- 01 as cited in the QAP. The RPDs are calculated for duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits. However, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPD is greater than 20%. The duplicate results were within a 20% RPD. Results of the RPD test are provided in Tab H. 3.4.6 Other Laboratory QA/QC Section 9.2 of the QAP requires that the laboratory's QA/QC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate Analytical Laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, EFRI' s QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided in Tab H. The lab QA/QC results met these specified acceptance limits. The QAP Section 8.1.2 requires that a Matrix Spike/Matrix Spike Duplicate ("MS/MSD") pair be analyzed with each analytical batch. The QAP does not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the MS/MSD pair be prepared on EFRI samples only. Acceptance limits for MS/MSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the QAP requirement to analyze an MS/MSD pair with each analytical batch was met. While the QAP does not require it, the recoveries were reviewed for compliance with the laboratory established acceptance limits. The QAP does not require this level of review, and the results of this review are provided for information only. The information from the Laboratory QA/QC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for the samples were within acceptable laboratory limits for the regulated compounds except as indicated in Tab H. The MS/MSD recoveries that are outside the laboratory established acceptance limits do not affect the quality or usability of the data because recoveries above or below the acceptance limits are indicative of matrix interference. Matrix interferences are applicable to the individual sample results only. The requirement in the 9 QAP to analyze a MS/MSD pair with each analytical batch was met and as such the data are compliant with the QAP. The information from the Laboratory QA/QC Summary Reports indicates that the Laboratory Control Sample recoveries were acceptable, which indicate that the analytical system was operating properly. The QAP Section 8.1.2 requires that each analytical batch shall be accompanied by a reagent blank. All analytical batches routinely contain a blank, which is a laboratory-grade water blank sample made and carried through all analytical steps. For the Mill samples, a method blank is prepared for all analytical methods. The information from the Laboratory QA/QC Summary Reports indicates that the method blanks did not contain detections of any target analytes above the Reporting Limit. 3.4. 7 Receipt Temperature Evaluation Chain of Custody sheets were reviewed to confirm compliance with the QAP requirement in QAP Table 1 that samples be received at 6°C or lower. Sample temperatures checks are provided in Tab H. All samples were received within the required temperature limit. 3.4.8 Rinsate Check Rinsate checks are provided in Tab H. A comparison of the rinsate blank sample concentration levels to the QAP requirements -that rinsate sample concentrations be one order of magnitude lower than that of the actual well -indicated that all of the rinsate blank analytes met this criterion. All rinsate and DIFB blank samples were non-detect for the quarter. 4.0 INTERPRETATIONOFDATA 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions. 4.1.1 Current Site Groundwater Contour Map As stated above, a listing of groundwater level readings for the current quarter (shown as depth to groundwater in feet) is included under Tab C. The data from this tab has been interpreted (interpolated by kriging) and plotted in a water table contour map, provided under the same tab. The contour map is based on the current quarter's data for all wells. The water level contour map indicates that perched water flow ranges from generally southwesterly beneath the Mill site and tailings cells to generally southerly along the eastern and western margins of White Mesa. Perched water mounding associated with the wildlife ponds locally changes the generally southerly perched water flow patterns. For example, northeast of the Mill site, mounding associated with wildlife ponds results in locally northerly flow near PIEZ-1. The impact of the mounding associated with the northern ponds, to which water has not been delivered since March 2012, is diminishing and is expected to continue to diminish as the mound decays due to reduced recharge. 10 Not only has recharge from the wildlife ponds impacted perched water elevations and flow directions at the site, but the cessation of water delivery to the northern ponds, which are generally upgradient of the nitrate and chloroform plumes at the site, has resulted in changing conditions that are expected to impact constituent concentrations and migration rates within the plumes. Specifically, past recharge from the ponds has helped limit many constituent concentrations within the plumes by dilution while the associated groundwater mounding has increased hydraulic gradients and contributed to plume migration. Since use of the northern wildlife ponds ceased in March 2012, the reduction in recharge and decay of the associated groundwater mound are expected to increase many constituent concentrations within the plumes while reducing hydraulic gradients and acting to reduce rates of plume migration. EFRI and its consultants have raised the issues and potential effects associated with cessation of water delivery to the northern wildlife ponds during discussions with DRC in March 2012 and May 2013. The impacts associated with cessation of water delivery to the northern ponds are expected to propagate downgradient (south and southwest) over time. Wells close to the ponds are generally expected to be impacted sooner than wells farther downgradient of the ponds. Therefore, constituent concentrations are generally expected to increase in downgradient wells close to the ponds before increases are detected in wells farther downgradient of the ponds. Although such increases are anticipated to result from reduced dilution, the magnitude and timing of the increases are difficult to predict due to the complex permeability distribution at the site and factors such as pumping and the rate of decay of the groundwater mound. The potential exists for some wells completed in higher permeability materials to be impacted sooner than some wells completed in lower permeability materials even though the wells completed in lower permeability materials may be closer to the ponds. Localized increases in concentrations of constituents such as nitrate and chloride within and near the nitrate plume may occur even when the nitrate plume is under control based on the Nitrate CAP requirements. Ongoing mechanisms that can be expected to increase the concentrations of nitrate and chloride locally as a result of reduced wildlife pond recharge include but are not limited to: 1) Reduced dilution -the mixing of low constituent concentration pond recharge into existing perched groundwater will be reduced over time. 2) Reduced saturated thicknesses -dewatering of higher permeability zones rece1vmg primarily low constituent concentration pond water will result in wells intercepting the zones receiving a smaller proportion of the low constituent concentration water. The combined impact of the above two mechanisms may be especially evident at chloroform pumping wells MW-4, MW-26, TW4-4, TW4-19, and TW4-20; nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2; and non-pumped wells adjacent to the pumped wells. The overall impact is expected to be generally higher constituent concentrations in these wells over the short term until mass reduction resulting from pumping and natural attenuation eventually reduce concentrations. In addition to changes in the flow regime caused by reduced wildlife pond recharge, perched flow directions are locally influenced by operation of the chloroform and nitrate pumping wells. 11 As shown in the detail water level map provided under Tab C, well defined cones of depression are evident in the vicinity of all chloroform pumping wells except TW4-4, which began pumping in the first quarter of 2010. Although operation of chloroform pumping well TW4-4 has depressed the water table in the vicinity of TW4-4, a well-defined cone of depression is not clearly evident. The lack of a well-defined cone of depression near TW4-4likely results from 1) variable permeability conditions in the vicinity of TW 4-4, and 2) persistent relatively low water levels at adjacent well TW4-14. Pumping of nitrate wells TW4-22, TW4-24, TW4-25, and TWN-2 began during the first quarter of 2013. Water level patterns near these wells are expected to be influenced by the presence of and the decay of the groundwater mound associated with the northern wildlife ponds, and by the persistently low water level elevation at TWN-7, which is located upgradient of the nitrate pumping wells. Capture associated with nitrate pumping is expected to increase over time as water levels decline due to pumping and to cessation of water delivery to the northern wildlife ponds. Interaction between nitrate and chloroform pumping is expected to enhance the capture of the nitrate pumping system. The long term interaction between the nitrate and chloroform pumping systems will, however, require more data to be collected as part of routine monitoring. As discussed above, variable permeability conditions are one likely reason for the lack of a well- defined cone of depression near chloroform pumping well TW 4-4. Changes in water levels at wells immediately south of TW4-4 resulting from TW4-4 pumping are expected to be muted because TW4-4 is located at a transition from relatively high to relatively low permeability conditions south (downgradient) of TW4-4. The permeability of the perched zone at TW4-6 and TW4-26, recently installed wells TW4-29, TW4-30, TW4-31, TW4-33, and TW4-34, and new well TW4-35 is one to two orders of magnitude lower than at TW4-4. Any drawdown of water levels at wells immediately south of TW4-4 resulting from TW4-4 pumping is also difficult to determine because of the general, long-term increase in water levels in this area due to recharge from the wildlife ponds. Water levels at TW4-4 and TW4-6 increased by nearly 2.7 and 2.9 feet, respectively, between the fourth quarter of 2007 and the fourth quarter of 2009 Gust prior to the start of TW 4-4 pumping) at rates of approximately 1.2 feet/year and 1.3 feet/year, respectively. However, the rate of increase in water level at TW4-6 after the start of pumping at TW4-4 (first quarter of 2010) was reduced to less than 0.5 feet/year suggesting that TW4-6 is within the hydraulic influence ofTW4-4. Furthermore, water levels at TW4-6 have been trending downward since the fourth quarter of 2013 suggesting an additional influence related to the cessation of water delivery to the nmthern wildlife ponds as discussed above. (note: hydrographs for these wells are provided in the quarterly Chloroform Monitoring Report). Recharge from the southern wildlife pond is expected to continue to have an effect on water levels near TW 4-4 even as the groundwater mound associated with recharge from the northern ponds diminishes over time due to cessation of water delivery to those ponds. The lack of a well-defined cone of depression at TW4-4 is also influenced by the persistent, relatively low water level at non-pumping well TW4-14, located east ofTW4-4 and TW4-6. For the current quarter, the water level at TW4-14 was measured at approximately 5530.4 feet above 12 mean sea level ("ft amsl"). This is approximately 8 feet lower than the water level at TW 4-6 (approximately 5538.7 ft amsl) and 13 feet lower than the water level at TW4-4 (approximately 5543.7 ft amsl) even though TW4-4 is pumping. Well TW4-27 (installed south of TW4-14 in the fourth quarter of 2011) has a static water level of approximately 5527.8 ft amsl, similar to TW4-14 (approximately 5530.4 ft amsl). TW4-27 was positioned at a location considered likely to detect any chloroform present and/or to bound the chloroform plume to the southeast and east (respectively) of TW4-4 and TW4-6. As will be discussed below, groundwater data collected since installation indicates that TW 4-27 does indeed bound the chloroform plume to the southeast and east of TW 4-4 and TW 4-6 (respectively); however chloroform exceeding 70 f.!g/L has been detected at recently installed temporary perched wells TW4-29 (located south of TW4-27) and TW4-33 (located between TW4-4 and TW4-29). The lack of a well-defined cone of depression at TW4-4 is also influenced by the persistent, relatively low water level at non-pumping well TW4-14, located east ofTW4-4 and TW4-6. For the current quarter, the water level at TW4-14 was measured at approximately 5530.4 feet above mean sea level ("ft amsl"). This is approximately 8 feet lower than the water level at TW4-6 (approximately 5538.7 ft amsl) and 13 feet lower than the water level at TW4-4 (approximately 5543.7 ft amsl) even though TW4-4 is pumping. Well TW4-27 (installed south of TW4-14 in the fourth quarter of 2011) has a static water level of approximately 5527.8 ft amsl, similar to TW4-14 (approximately 5530.4 ft amsl). Prior to the installation of TW4-27, the persistently low water level at TW4-14 was considered anomalous because it appeared to be downgradient of all three wells TW4-4, TW4-6, and TW4-26, yet chloroform had not been detected at TW4-14. Chloroform had apparently migrated from TW4-4 to TW4-6 and from TW4-6 to TW4-26 which suggested that TW4-26 was actually downgradient of TW4-6, and TW4-6 was actually downgradient of TW4-4, regardless of the flow direction implied by the low water level at TW4-14. The water level at TW4-26 (5537.1 feet amsl) is, however, lower than water levels at adjacent wells TW4-6 (5538.7 feet amsl), and TW4-23 (5540.3 feet amsl), as shown in the detail water level map under Tab C. Hydraulic tests indicate that the permeability at TW4-27 is an order of magnitude lower than at TW4-6 and three orders of magnitude lower than at TW4-4 (see Hydro Geo Chern, Inc. [HGC], September 20, 2010: Hydraulic Testing of TW4-4, TW4-6, and TW4-26, White Mesa Uranium Mill, July 2010; and HGC, November 28, 2011: Installation, Hydraulic Testing, and Perched Zone Hydrogeology of Perched Monitoring Well TW4-27, White Mesa Uranium Mill Near Blanding, Utah). The similar water levels at TW4-14 and TW4-27, and the low permeability estimate at TW4-27 suggest that both wells are completed in materials having lower permeability than nearby wells. The low permeability condition likely reduced the rate of long-term water level increase at TW4-14 and TW4-27 compared to nearby wells, yielding water levels that appeared anomalously low. This behavior is consistent with hydraulic test data collected from recently installed wells TW4-29, TW4-30, TW4-31, TW4-33 and TW4-34 which indicate that the permeability of these wells is one to two orders of magnitude higher than the permeability of TW4-27 (see HGC, January 23, 2014; Contamination Investigation Report, TW4-12 and TW4- 27 Areas, White Mesa Uranium Mill Near Blanding, Utah; and HGC, July 1, 2014, Installation and Hydraulic Testing of TW4-35 and TW4-36, White Mesa Uranium Mill Near Blanding, Utah 13 [As-Built Report]). Hydraulic tests also indicate that the permeability at TW4-36 is slightly higher than but comparable to the low permeability at TW4-27, suggesting that TW4-36, TW4- 14 and TW4-27 are completed in a continuous low permeability zone. 4.1.2 Comparison of Current Groundwater Contour Map to Groundwater Contour Map for Previous Quarter The groundwater contour maps for the Mill site for the previous quarter, as submitted with the Nitrate Monitoring Report for the previous quarter, are attached under Tab D. A comparison of the water table contour maps for the current quarter (fourth quarter of 2014) to the water table contour maps for the previous quarter (third quarter of 2014) indicates slightly larger drawdowns related to operation of chloroform pumping wells MW-26and TW4-20 and nitrate pumping well TW4-25. Nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2 were brought into operation during the first quruter of 2013 and their impact on water level patterns was evident as of the fourth quarter of 2013. While water levels in nitrate pumping wells TW4-22, TW4-24, and TW4-25 showed decreases, the water level at TWN-2 showed an increase this quarter. As discussed in Section 4.1.1, pumping at chloroform well TW 4-4, which began in the first quarter of 2010, has depressed the water table near TW4-4, but a well-defined cone of depression is not clearly evident, likely due to variable permeability conditions near TW4-4 and the persistently low water level at adjacent well TW4-14. Small ( <1 foot) changes in water levels were reported at the majority of site wells; water levels and water level contours for the site have not changed significantly since the last quarter except for a few locations. Reported decreases in water levels (increases in drawdown) of approximately 3.4, 1.6, 1.4, 2.5, and 2.8 feet occurred in chloroform pumping wells MW-26 and TW4-20, and nitrate pumping wells TW4-22, TW4-24, and TW4-25, respectively. An increase in water level (decrease in drawdown) of approximately 5 feet was reported for nitrate pumping well TWN-2. Changes in water levels at other pumping wells (chloroform pumping wells MW -4, TW 4-4, and TW 4-19 were less than 1 foot. Water level fluctuations at pumping wells typically occur in part because of fluctuations in pumping conditions just prior to and at the time the measurements are taken. Although decreases in water levels (decreases in drawdown) occuued at chloroform pumping wells MW-26 and TW4-20, and nitrate pumping wells TW4-22, TW4-24, and TW4-25 the apparent capture of these wells relative to other pumping wells has increased in some cases and decreased in others, while the overall capture of the combined pumping systems has increased slightly. Reported water level decreases of less than 1 foot at Piezometers 1 through 3, TWN-1, TWN-4, TWN-6, TWN-18, and MW-19 may result from cessation of water delivery to the northern wildlife ponds as discussed in Section 4.1.1 and the consequent continuing decay of the associated perched water mound. Reported water level decreases of approximately 0.6 feet and 0.7 feet at Piezometers 4 and 5 may result from reduced recharge at the southern wildlife pond. 14 Reported water levels decreased by approximately 4.3 feet at MW-20 and increased by approximately 4.8 feet at MW-37 between the previous quarter and the current quarter. Water level variability at these wells is likely the result of low permeability and variable intervals between purging/sampling and water level measurement. A decrease in water level of approximately 2.9 feet and increases of approximately 2.4 feet and 2.9 feet were reported at DR- 17, MW-23 and TW4-21, respectively. 4.1.3 Hydrographs Attached under Tab E are hydrographs showing groundwater elevation in each nitrate contaminant investigation monitor well over time. Per the CAP, nitrate wells TWN-6, TWN-14, TWN-16, and TWN-19 have been maintained for depth to groundwater monitoring only. These hydrographs are also included in Tab E. 4.1.4 Depth to Groundwater Measured and Groundwater Elevation Attached in Tab F are tables showing depth to groundwater measured and groundwater elevation over time for each of the wells listed in Section 2.1.1 above. 4.2 Effectiveness of Hydraulic Containment and Capture 4.2.1 Hydraulic Containment and Control The CAP states that hydraulic containment and control will be evaluated in part based on water level data and in part on concentrations in wells downgradient of pumping wells TW4-22 and TW4-24. As per the CAP, the fourth quarter of 2013 was the first quarter that hydraulic capture associated with nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2 was evaluated. Hydraulic containment and control based on water level data is considered successful per the CAP if the entire nitrate plume up gradient of TW 4-22 and TW 4-24 falls within the combined capture of the nitrate pumping wells. Capture zones based on water level contours calculated by kriging the current quarter's water level data are provided on water level contour maps included under Tab C. The nitrate capture zones are defined by the bounding stream tubes associated with nitrate pumping wells. Each bounding stream tube represents a flow line parallel to the hydraulic gradient and therefore perpendicular to the intersected water level contours. Assuming that the stream tubes do not change over time, all flow between the bounding stream tubes associated with a particular pumping well is presumed to eventually reach and be removed by that well. Capture associated with chloroform pumping wells is also included on these maps because the influence of the chloroform and nitrate pumping systems overlap. The specific methodology for calculating the nitrate capture zones is substantially the same as that used since the fourth quarter of 2005 to calculate the capture zones for the chloroform program, as agreed to by the DRC and International Uranium (USA) Corp. The procedure for calculating nitrate capture zones is as follows: 15 1) Calculate water level contours by gridding the water level data on approximately 50-foot centers using the ordinary linear kriging method in Surfer™. Default kriging parameters are used that include a linear variogram, an isotropic data search, and all the available water level data for the quarter, including relevant seep and spring elevations. 2) Calculate the capture zones by hand from the kriged water level contours following the rules for flow nets: -from each pumping well, reverse track the stream tubes that bound the capture zone of each well, -maintain perpendicularity between each stream tube and the kriged water level contours. Compared to last quarter, reported changes in water levels at nitrate pumping wells other than TWN-2 were less than three feet, as were the reported water level changes at chloroform pumping wells other than MW-26. A large increase of approximately 5 feet was reported for nitrate pumping well TWN-2, and a decrease of approximately 3.4 feet was reported for chloroform pumping well MW-26. Overall, the apparent capture of the combined nitrate and chloroform pumping systems has increased slightly since last quarter. The capture associated with nitrate pumping wells is expected to increase over time as water levels continue to decline due to pumping and to cessation of water delivery to the northern wildlife ponds. Slow development of hydraulic capture is consistent with and expected based on the relatively low permeability of the perched zone at the site. Furthermore, the presence of the perched groundwater mound, and the apparently anomalously low water level at TWN-7, will influence the definition of capture associated with the nitrate pumping system. That pumping is likely sufficient to eventually capture the entire plume upgradient of TW4-22 and TW4-24 can be demonstrated by comparing the combined average pumping rates of all nitrate pumping wells for the current quarter to estimates of pre-pumping flow through the nitrate plume near the locations of TW4-22 and TW4-24. The pre-pumping flow calculation is assumed to represent a steady state 'background' condition that includes constant recharge, hydraulic gradients, and saturated thicknesses, and does not account for reduced recharge and saturated thickness caused by cessation of water delivery to the northern wildlife ponds since March, 2012. Changes after pumping are conservatively assumed to result only from pumping. As will be discussed below, the average combined nitrate pumping rate for the quarter is approximately the same as, to a factor approximately 2.1 times greater than, the calculated pre-pumping rate of perched water flow through the nitrate plume. The cumulative volume of water removed by TW4-22, TW4-24, TW4-25, and TWN-2 during the current quarter was approximately 357,427 gallons. This equates to an average total extraction rate of approximately 2.7 gpm over the 92 day quarter. This average accounts for time periods when pumps were off due to insufficient water columns in the wells. Pre-pumping flow through the nitrate plume near TW4-22 and TW4-24 was estimated using Darcy's Law to lie within a range of approximately 1.31 gpm to 2.79 gpm. Calculations were based on an average hydraulic conductivity range of 0.15 feet per day (ft/day) to 0.32 ft/day (depending on the calculation method), a pre-pumping hydraulic gradient of 0.025 feet per foot 16 (ft/ft), a plume width of 1,200 feet, and a saturated thickness (at TW4-22 and TW4-24) of 56 feet. The hydraulic conductivity range was estimated by averaging the results obtained from slug test data that were collected automatically by data loggers from wells within the plume and analyzed using the KGS unconfined slug test solution available in Aqtesolve™ (see Hydro Geo Chern, Inc. [HGC], August 3, 2005: Perched Monitoring Well Installation and Testing at the White Mesa Uranium Mill, April Through June 2005; HGC, March 10, 2009: Perched Nitrate Monitoring Well Installation and Hydraulic Testing, White Mesa Uranium Mill; and HGC, March 17 2009: Letter Report to David Frydenlund, Esq, regarding installation and testing of TW4-23, TW4-24, and TW4-25). These results are summarized in Table 6. Data from fourth quarter 2012 were used to estimate the pre-pumping hydraulic gradient and saturated thickness. These data are also summarized in Tables 7 and 8. The average hydraulic conductivity was estimated to lie within a range of 0.15 ft/day to 0.32 ft/day. Averages were calculated four ways. As shown in Table 6 arithmetic and geometric averages for wells MW-30, MW-31, TW4-22, TW4-24, TW4-25, TWN-2, and TWN-3 were calculated as 0.22 and 0.15 ft/day, respectively. Arithmetic and geometric averages for a subset of these wells (MW-30, MW-31, TW4-22, and TW4-24) were calculated as 0.32 and 0.31 ft/day, respectively. The lowest value, 0.15 ft/day, represented the geometric average of the hydraulic conductivity estimates for all the plume wells. The highest value, 0.32 ft/day, represented the arithmetic average for the four plume wells having the highest hydraulic conductivity estimates (MW-30, MW-31, TW4-22, and TW4-24). Pre-pumping hydraulic gradients were estimated at two locations; between TW4-25 and MW-31 (estimated as 0.023 ft/ft), and between TWN-2 and MW-30 (estimated as 0.027 ft/ft). These results were averaged to yield the value used in the calculation (0.025 ft/ft). The pre-pumping saturated thickness of 56 feet was an average of pre-pumping saturated thicknesses at TW4-22 and TW4-24. The hydraulic gradient and saturated thickness used in the calculations are assumed to represent a steady state 'background' condition. However, assumption of a steady state 'background' is inconsistent with the cessation of water delivery to the northern wildlife ponds, located upgradient of the nitrate plume. Hydraulic gradients and saturated thicknesses within the plume are declining as a result of two factors: reduced recharge from the ponds, and the effects of nitrate pumping. Separating the impacts of nitrate pumping from the impacts of reduced recharge from the ponds is problematic. Should pumping cease and 'background' conditions be allowed to re-establish, however, smaller hydraulic gradients and saturated thicknesses would be expected due to reduced recharge, which would lower estimates of 'background' flow. As a result, the 'background' flow calculated using the hydraulic gradient of 0.025 ft/ft and saturated thickness of 56 feet is considered conservatively large. Furthermore, using the arithmetic average hydraulic conductivity of a subset of plume wells having the highest conductivities is considered less representative of actual conditions than using the geometric average conductivity of all of the plume wells. Nitrate pumping may therefore exceed flow through the plume by a factor greater than 2.1, the high end of the calculated range. The CAP states that MW-5, MW-11, MW-30, and MW-31 are located downgradient ofTW4-22 and TW4-24. MW-30 and MW-31 are within the plume near its downgradient edge and MW-5 17 and MW -11 are outside and downgradient of the plume. Per the CAP, hydraulic control based on concentration data will be considered successful if the concentrations of nitrate in MW-30 and MW -31 remain stable or decline, and concentrations of nitrate in downgradient wells MW -5 and MW -11 do not exceed the 10 mg/L standard. Table 5 presents the nitrate concentration data for MW-30, MW-31, MW-5 and MW-11, which are down-gradient of pumping wells TW4-22 and TW4-24. Based on these concentration data, the nitrate plume is under control. The plume has not migrated downgradient to MW -5 or MW -11 because the nitrate concentration at MW-5 is approximately 0.2 mg/L this quarter and nitrate was not detected at MW-11. Between the previous and current quarters, nitrate concentrations increased in both MW-30 and MW-31. Nitrate in MW-30 increased from 13.8 mg/L to 16.2 mg/L and nitrate in MW-31 increased from 15.2 mg/L to 20.9 mg/L. Although short-term fluctuations have occurred, nitrate concentrations in MW-30 and MW-31 have been relatively stable, demonstrating that plume migration is minimal or absent. Chloride has been relatively stable at MW-30 but is increasing at MW-31 (see Tab J and Tab K, discussed in Section 4.2.4). The apparent increase in chloride and stable nitrate at MW-31 suggests a natural attenuation process that is affecting nitrate but not chloride. A likely process that would degrade nitrate but leave chloride unaffected is reduction of nitrate by pyrite. The likelihood of this process in the perched zone is discussed in HGC, December 7 2012; Investigation of Pyrite in the Perched Zone, White Mesa Uranium Mill Site, Blanding, Utah. 4.2.2 Current Nitrate and Chloride Isoconcentration Maps Included under Tab I of this Report are current nitrate and chloride iso-concentration maps for the Mill site. Nitrate iso-contours start at 5 mg/L and chloride iso-contours start at 100 mg/L because those values appear to separate the plumes from background. All nitrate and chloride data used to develop these iso-concentration maps are from the current quarter's sampling events. 4.2.3 Comparison of Areal Extent Increases in nitrate concentrations in most wells within the nitrate plume since last quarter have resulted in a slight expansion of the plume area. The concentration in TWN-3 decreased from approximately 20 mg/L to 19 mg/L; the concentration in MW-30 increased from approximately 14 mg/L to 16 mg/L; and the concentration in MW-31 increased from approximately 15 mg/L to 21 mg/L. The concentration in nitrate pumping well TWN-2 increased from approximately 42 mg/L to 71 mg/L; the concentration in nitrate pumping well TW4-22 increased from approximately 42 mg/L to 55 mg/L; and the concentration in nitrate pumping well TW4-24 increased from approximately 32 mg/L to 36 mg/L. In addition, the concentration in TW4-21 increased from 7.1 mg/L last quarter to 10 mg/L this quarter, bringing it again just within the nitrate plume boundary. (see Tab J and Tab K, discussed in Section 4.2.4). The nitrate concentration at TW4-18 (located east of the nitrate plume) increased from 9.8 mg/L to 11.1 mg/L after decreasing for the previous three quarters. Changes in nitrate concentrations near TW 4-18 are expected to result from changes in pumping and from the cessation of water 18 delivery to the northern wildlife ponds. The reduction in low-nitrate recharge from the ponds appeared to be having the anticipated effect of generally increased nitrate concentrations in wells downgradient of the ponds. However, decreasing nitrate concentrations at most wells in the vicinity of TW4-18 over the previous three quarters after previous increases suggests that conditions in this area have stabilized. Although increases in concentration in the area downgradient of the wildlife ponds have been anticipated as the result of reduced dilution, the magnitude and timing of the increases are difficult to predict due to the measured variations in hydraulic conductivity at the site and other factors. Nitrate in the area directly downgradient (south to south-southwest) of the northern wildlife ponds is associated with the chloroform plume, is cross-gradient of the nitrate plume as defined in the CAP, and is within the capture zone of the chloroform pumping system (primarily chloroform pumping well MW-26). Perched water flow in the area is to the southwest in the same approximate direction as the main body of the nitrate plume. Nitrate concentrations at the downgradient edge of the plume (MW-30 and MW-31) continue to be relatively stable, demonstrating that plume migration is minimal or absent. With regard to chloroform, since the initiation of nitrate pumping, the boundary of the chloroform plume has migrated to the west toward nitrate pumping well TW4-24, and more recently has migrated to the southwest to reincorporate chloroform monitoring wells TW4-6 and TW4-16. More details regarding the chloroform data and interpretation are included in the Quarterly Chloroform Monitoring Report submitted under separate cover. 4.2.4 Nitrate and Chloride Concentration Trend Data and Graphs Attached under Tab J is a table summarizing values for nitrate and chloride for each well over time. Attached under Tab K are graphs showing nitrate and chloride concentration plots in each monitor well over time. 4.2.5 Interpretation of Analytical Data Comparing the nitrate analytical results to those of the previous quarter, as summarized in the tables included under Tab J, the following observations can be made for wells within and immediately surrounding the nitrate plume: a) Nitrate concentrations have increased by more than 20% in the following wells compared to last quarter: MW-26, MW-27, MW-31, TW4-10, TW4-16, TW4-19, TW4- 20, TW4-21, TW4-22, and TWN-2; b) Nitrate concentrations have decreased by more than 20% in the following wells compared to last quarter: TW4-25 and TWN-4; c) Nitrate concentrations have remained within 20% in the following wells compared to last quarter: MW-30, TW4-5, TW4-18, TW4-24, TWN-1, TWN-3, TWN-7 and TWN- 18;and d) MW-11, MW-25, and MW-32 remained non-detect 19 As indicated, nitrate concentrations for many of the wells with detected nitrate were within 20% of the values reported during the previous quarter, suggesting that variations are within the range typical for sampling and analytical error. The remaining wells had changes in concentration greater than 20%. The latter includes chloroform pumping wells MW-26, TW4-19, and TW4-20; nitrate pumping wells TW4-22, TW4-25 and TWN-2; and non-pumping wells MW-27, MW-31, TW4-10, TW4-16, TW4-21, and TWN-4. TW4-10 and TW4-16 are located adjacent to chloroform pumping well MW-26; TW4-21 is located adjacent to chloroform pumping well TW4-19; and TWN-4 is located between the northern wildlife ponds and nitrate pumping wells TW4-25 and TWN-2. Fluctuations in concentrations at pumping wells and wells adjacent to pumping wells likely result in part from the effects of pumping as discussed in Section 4.1.1. Concentrations at TW4-21 are also influenced by its location near the eastern nitrate and northern chloroform plume boundaries. MW -31 is located in the downgradient portion of the nitrate plume and is expected to be influenced by changes in upgradient pumping at nitrate pumping wells TW4-22 and TW4-24 and chloroform pumping wells MW-26, TW4-19 and TW4-20. As discussed in Section 4.2.3, the nitrate concentration at TW4-21 increased from 7.1 mg/L last quarter to 10 mg/L this quarter, bringing it again just within the nitrate plume boundary. The nitrate concentration in nitrate pumping well TW4-25 decreased from approximately 1.6 mg/L last quarter to 1.0 mg/L this quarter. The nitrate concentrations in chloroform pumping wells MW-26, TW4-19, and TW4-20 increased from approximately 0.7 mg/L, 1.6 mg/L and 4.3 mg/L, respectively, to approximately 1.1 mg/L, 4.7 mg/L, and 7.7 mg/L. The chloroform concentration at nitrate pumping well TW4-24 decreased from 76.3 ~-tg/L to 25.8 ~-tg/L. The decrease at TW4- 24 pushed the chloroform plume boundary back to the east of TW4-24; last quarter, a chloroform concentration increase from 62.7 ~-tg/L to 76.3 ~-tg!L moved the chloroform plume boundary to the west of TW4-24. Chloroform changes at TW4-22 and TW4-24 are likely in response to the start-up of nitrate pumping in the first qumter of 2013 and are affected by the presence of historically high chloroform concentrations at adjacent, cross-gradient well TW4-20. MW-27, located west of TWN-2, and TWN-18, located north of TWN-3, bound the nitrate plume to the west and north (See Figure I-1 under Tab I). In addition, the southernmost (downgradient) boundary of the plume remains between MW-30/MW-31 and MW-5/MW-11. Nitrate concentrations at MW-5 (adjacent to MW-11) and MW-11 have historically been low(< 1 mg/L) or non-detect for nitrate (See Table 5). MW-25, MW-26, MW-32, TW4-16, TW4-19, TW4-20, TW4-25, TWN-1, and TWN-4 bound the nitrate plume to the east. As discussed above, the areal extent of the plume has expanded slightly, with the plume boundaries moving outward in some areas, primarily due to increases in concentrations at wells within the plume. Nitrate concentrations outside the nitrate plume exceed 10 mg/L at a few locations: TW4-12 (16.1 mg/L), TW4-26 (12.3 mg/L), TW4-27 (28.2 mg/L), and TW4-28 (16.5 mg/L). All these wells are located southeast of the nitrate plume as defined in the CAP and all are separated from the plume by wells having nitrate concentrations that are either non-detect, or, if detected, are less than 10 mg/L. Concentrations at TW4-26, TW4-27 and TW4-28 are within 20% of their concentrations during the previous quarter, while the concentration at TW 4-12 increased more than 20%, from approximately 13 mg/L to 16 mg/L. From the third quarter of 2013 through the second quarter of 2014, nitrate concentrations at TW4-10 and TW4-18 exceeded 10 mg/L. Although last quarter, nitrate concentrations at both TW4-10 and TW4-18 20 decreased to 9.8 mg/L, both are again above 10 mg/L this quarter. Elevated nitrate concentrations at these wells are associated with the chloroform plume, and both are within the capture zone of the chloroform pumping system. Elevated nitrate at TW4-12, TW4-26, TW4-27, and TW4-28 is likely related to former cattle ranching operations at the site. Chloride concentrations are measured because elevated chloride (greater than 100 mg/L) is associated with the nitrate plume. Chloride concentrations at all sampled locations this quarter are within 20% of their respective concentrations during the previous quarter. Although changes were within 20%, more increases were detected than decreases. Increases in concentrations at wells near (and downgradient of) the northern wildlife ponds are anticipated as a result of reduced dilution caused by cessation of water delivery to the northern wildlife ponds. 4.3 Estimation of Pumped Nitrate Mass and Residual Nitrate Mass within the Plume Nitrate mass removed by pumping is summarized in Table 2, and includes mass removed by both chloroform and nitrate pumping wells. Table 3 shows the volume of water pumped at each well and Table 4 provides the details of the nitrate removal for each well. Mass removal calculations begin with the third quarter of 2010 because the second quarter, 2010 data were specified to be used to establish a baseline mass for the nitrate plume. As stated in the CAP, the baseline mass is to be calculated using the second quarter, 2010 concentration and saturated thickness data "within the area of the kriged 10 mg!L plume boundary." The second quarter, 2010 data set was considered appropriate because "the second quarter, 2010 concentration peak at TWN-2 likely identifies a high concentration zone that still exists but has migrated away from the immediate vicinity of TWN-2." As shown in Table 2, a total of approximately 1,173 lb of nitrate has been removed from the perched zone since the third quarter of 2010. Prior to the first quarter of 2013, all direct nitrate mass removal resulted from operation of chloroform pumping wells MW-4, MW-26, TW4-4, TW4-19, and TW4-20. During the current quarter: • A total of approximately 109 lb of nitrate was removed by the chloroform pumping wells and by nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2. • Of the 109 lb removed during the current quatter, approximately 93 lb, (or 85 %), was removed by the nitrate pumping wells. Baseline mass and current quarter mass estimates (nitrate + nitrite as N) for the nitrate plume are approximately 43,700 lb and 34,370 lbs, respectively. Mass estimates were calculated within the plume boundaries as defined by the kriged 10 mg!L isocon by 1) gridding (kriging) the nitrate concentration data on 50-foot centers; 2) calculating the volume of water in each grid cell based on the saturated thickness and assuming a porosity of 0.18; 3) calculating the mass of nitrate+nitrite as N in each cell based on the concentration and volume of water for each cell; and 4) totaling the mass of all grid cells within the 10 mg/L plume boundary. Data used in these calculations included data from wells listed in Table 3 of the CAP. The nitrate mass estimate for the current quarter is lower than the baseline estimate by 9,330 lb, and this difference is greater than the amount of nitrate mass removed directly by pumping. Changes in the quarterly mass estimates are expected to result primarily from 1) nitrate mass 21 removed directly by pumping, 2) natural attenuation of nitrate, and 3) changes in nitrate concentrations in wells within the plume as a result of re-distribution of nitrate within the plume and changes in saturated thicknesses. Redistribution of nitrate within the plume and changes in saturated thicknesses will be impacted by changes in pumping and in background conditions such as the decay of the perched water mound associated with the northern wildlife ponds. Cessation of water delivery to the northern wildlife ponds is expected to result in reduced saturated thicknesses and reduced dilution, which in turn is expected to result in increases in concentrations. The mass estimate during the current quarter (34,370 lb) was larger than the mass estimate during the previous quarter (24,140 lb) by 10,230 lb or 42 %. This difference results from higher nitrate concentrations measured in most wells within the plume and the resulting increased areal extent this quarter compared to last quarter. Nitrate mass removal by pumping and natural attenuation (expected to result primarily from pyrite oxidation/nitrate reduction) act to lower nitrate mass within the plume. Changes resulting from redistribution of nitrate within the plume are expected to result in both increases and decreases in concentrations at wells within the plume and therefore increases and decreases in mass estimates based on those concentrations, thus generating 'noise' in the mass estimates. Furthermore, because the sum of sampling and analytical error is typically about 20%, changes in the mass estimates from quarter to quarter of up to 20% could result from typical sampling and analytical error alone. Only longer-term analyses of the mass estimates that minimize the impacts of these quarter to quarter variations will provide useful information on plume mass trends. Over the long term, nitrate mass estimates are expected to trend downward as a result of direct removal by pumping and through natural attenuation. As specified in the CAP, once eight quarters of data have been collected (starting with the first quarter of 2013), a regression trend line is to be applied to the quarterly mass estimates and evaluated. The trend line will then be updated quarterly and reevaluated as additional quarters of data are collected. The evaluation will determine whether the mass estimates are increasing, decreasing, or stable. As the current quarter constitutes the eighth quarter as specified in the CAP, the mass estimates were plotted and a regression line fitted to the data, as shown in Figure M.1 of Tab M. The fitted line shows a decreasing trend in the mass estimates. As discussed above, the quarterly mass estimates are based on gridded (kriged) concentration data and saturated thicknesses (derived from gridded water level and base of perched zone data). Mass estimates are thus expected to depend primarily on wells within the plume having both relatively high concentrations and saturated thicknesses. An analysis of the relative influence of individual wells on the mass estimates was performed based on data from the eight wells originally within the plume (TWN-2, TWN-3, TW4-21, TW4-22, TW4-24, TW4-25, MW-30, and MW-31). Although TW4-21 has been both within and outside the plume, and TW4-25 is no longer within the plume, these wells were originally within the plume as defined in the CAP and were included in the analysis. Both are important due to their close proximities to the plume boundary. 22 Figures M.2 through M.9 are plots comparing the mass estimates to concentration, saturated thickness, and the product of concentration and saturated thickness (in units of pounds per square foot of plume [lbs/ft2]) at each well originally within the plume. Examination of these plots suggests that changes in concentration and in the product of concentration and saturated thickness at TWN-2 have the largest impact on changes in the mass estimates. This is reasonable because both concentrations and saturated thicknesses at TWN-2 are relatively large. Ten methods were used to quantitatively evaluate the relative influence of individual wells on the mass calculations. Well rankings derived from the ten methods are provided in Table M.l, with a rank of 1 indicating the greatest influence and a rank of 8 indicating the least influence. Methods 1, 2, and 3 rank each well based on the averages of concentration, saturated thickness, and product of concentration and saturated thickness, respectively. Averages were calculated from data over the last eight quarters (including the current quarter) and the baseline (second quarter, 2010) data. Methods 4, 5, 6, and 7 constitute sensitivity analyses using average concentration and saturated thickness data from the baseline (second quarter, 2010) data, and data from the last eight quarters (including the current quarter). These averages were used to compute an 'average plume' and 'average plume' mass estimate. Thirty two additional mass estimates were then computed by leaving out of the gridding process either the data from one of the original eight wells within the plume (method 4) or by modifying the data from one of the original eight wells within the plume. Data modification included: increasing the average nitrate concentration at a particular well by 20% (method 5); decreasing the average nitrate concentration at a particular well by 20% (method 6); and decreasing the average saturated thickness at a particular well by 20% (method 7). These methodologies automatically account for the variation in the lateral influence of individual wells, and the kriged plume boundaries are allowed to change based on the imposed changes. Methods 8, 9, and 10 constituted evaluation of the relative influence of each of the eight original wells on the kriged 'average plume'. A polygonal estimator was used to apportion the mass, volume, and average concentration associated with each well within the kriged average plume boundary. These methodologies also account for variations in the lateral influence of individual wells within the fixed 'average plume' boundary. Results of methods 1 through 3, 4 through 7, 8 through 10, and 3 and 8, were also scored collectively for overall rank. In each case, the score for a well consists of the sum of ranks for that well obtained by the indicated methods. Grouping of the methods were based on similarity. As discussed above, methods 1 through 3 rank influence based on raw concentration and saturated thickness data at individual wells and do not account for variable lateral influence of individual wells. Methods 4 through 10 rank influence based on gridded data and therefore account for variation in the lateral influence of wells. Methods 4 through 7 constitute sensitivity analyses; and methods 8 through 10 apportion mass, volume, and average concentration within the average kriged plume to individual wells using a polygonal estimator. Methods 3 and 8 are similar in that both rank influence based on the product of concentration and saturated thickness. Because method 8 ranks influence based on gridded data it additionally accounts for lateral influence. 23 The results of collectively scoring methods 1 through 3 are shown in Table M.2. The wells in order of importance are: TWN-2, TW4-22, MW-31, TW4-24, TWN-3, TW4-21ffW4-25, and MW-30. The results of collectively scoring methods 4 through 7 are shown in Table M.3. Wells in descending order of influence are: TWN-2, TW4-24/MW-31, TW4-22, MW-30, TW4-25, TWN- 3, and TW4-21. As indicated in Table M.1, rankings for methods 5, 6, and 7 were similar, with the top four consisting, in descending influence, of TW4-24, TWN-2, MW-31, and TW4-22. Method 4 ranked the top 4 wells as TWN-2, MW-30, MW-31, and TW4-22. The results of collectively scoring methods 8 through 10 are shown in Table M.4. Wells in descending order of influence are: TWN-2, TW4-22, MW-31, TW4-24, TWN-3, TW4-21/TW4- 25, and MW-30. As indicated in Table M.1, rankings for methods 8, 9, and 10 were similar with regard to the top 4 rankings; wells TWN-2, TW4-22, TW4-24, and MW-31 were in the top 4 of each method albeit in different order for each method. The top four (in descending influence) were for method 8: TW4-24, TWN-2, TW4-22, and MW-31; for method 9: TW4-24, TWN-2, MW-31, and TW4-22; and for method 10: TWN-2, TW4-22, TW4-24, and MW-31. The results of collectively scoring methods 3 and 8 are shown in Table M.5. The ranking of the top four consists (in descending order of influence) of TWN-2, TW4-24, TW4-22, and MW-31. The result of collectively scoring all methods is shown in Table M.6. Although this scoring lumps dissimilar methods, the results are similar to those obtained from the collective scoring of groups of similar methods described above. Well TWN-2 is ranked as having the most influence. The top four wells (in descending order of influence) are: TWN-2, TW4-24, MW-31, and TW4- 22. The results of the visual and quantitative analyses indicate that var1atwns in plume mass estimates can be expected to depend primarily on variations in data from TWN-2. Wells TW4- 22, TW4-24, and MW-31 (not necessarily in that order) are collectively the next most important with regard to influence on the mass estimates. 5.0 LONG TERM PUMP TEST AT TWN-02, TW4-22, TW4-24, and TW4- 25 OPERATIONS REPORT 5.1 Introduction Beginning in January 2013, EFRI began long term pumping of TW4-22, TW4-24, TW4-25, and TWN-02 as required by the Nitrate CAP, dated May 7, 2012 and the SCO dated December 12, 2012. In addition, as a part of the investigation of chloroform contamination at the Mill site, EFRI has been conducting a Long Term Pump Test on MW-4, TW4-19, MW-26, and TW4-20, and, since January 31, 2010, TW4-4. The purpose of the test is to serve as an interim action that will 24 remove a significant amount of chloroform-contaminated water while gathering additional data on hydraulic properties in the area of investigation. Because wells MW-4, TW4-19, MW-26, TW4-4 and TW4-20 are pumping wells that may impact the removal of nitrate, they are included in this report and any nitrate removal realized as part of this pumping is calculated and included in the quarterly reports. The following information documents the operational activities during the quarter. 5.2 Pumping Well Data Collection Data collected during the quarter included the following: • Measurement of water levels at MW-4, TW4-19, MW-26, and TW4-20 and, commencing regularly on March 1, 2010, TW4-4, on a weekly basis, and at selected temporary wells and permanent monitoring wells on a monthly basis. • Measurement of pumping history, including: pumping rates total pumped volume operational and non-operational periods. • Periodic sampling of pumped water for chloroform and nitrate/nitrite analysis and other constituents • Measurement of water levels weekly at TW4-22, TW4-24, TW4-25, and TWN-02 commencing January 28, 2013, and on a monthly basis selected temporary wells and permanent monitoring wells. 5.3 Water Level Measurements Beginning August 16, 2003, water level measurements from chloroform pumping wells MW-4, MW-26, and TW4-19 were conducted weekly. From commencement of pumping TW4-20, and regularly after March 1, 2010 for TW4-4, water levels in these two chloroform pumping wells have been measured weekly. From commencement of pumping in January 2013, water levels in wells TW4-22, TW4-24, TW4-25, and TWN-02 have been measured weekly. Copies of the weekly Depth to Water monitoring sheets for MW-4, MW-26, TW4-19, TW4-20, TW4-4, TW4- 22, TW4-24, TW4-25 and TWN-02 are included under Tab C. Monthly depth to water monitoring is required for all of the chloroform contaminant investigation wells and non-pumping wells MW-27, MW-30, MW-31, TW4-21, TWN-1, TWN- 3, TWN-4, TWN-7, and TWN-18. Copies of the monthly depth to Water monitoring sheets are included under Tab C. 5.4 Pumping Rates and Volumes The pumping wells do not pump continuously, but are on a delay device. The wells purge for a set amount of time and then shut off to allow the well to recharge. Water from the pumping wells is either transferred to the Cell 1 evaporation pond or is used in the Mill process. 25 The pumped wells are fitted with a flow meter which records the volume of water pumped from the well in gallons. The flow meter readings shown in Tab C are used to calculate the gallons of water pumped from the wells each quarter as required by Section 7 .2.2 of the CAP. The average pumping rates and quarterly volumes for each of the pumping wells are shown in Table 3. The cumulative volume of water pumped from each of the wells is shown in Table 4. Specific operational problems observed with the well or pumping equipment which occurred during the quarter are noted for each well below in Sections 5.4.1 through 5.4.4. The following two issues were noted as affecting multiple wells in the pumping network as and are not repeated under the Section for each well. On November 23, 2014, the Mill experienced a power outage resulting from high winds (in excess of 60+ mph) in the area. During the power outage all of the pumping wells (MW -04, TW4-04, MW-26, TW4-19, TW4-20, TW4-22, TW4-24, and TW4-25) ceased pumping. Power was partially restored to portions of the Mill on November 23, 2014 and power was fully restored to the entire Mill facility by 7:00AM November 24, 2014. Pumping of the chloroform wells was restored within 24-hours of discovery. No official notifications to DRC were required as the issue was rectified within 24-hours. DRC was notified by telephone that the issue was resolved within the 24-hour window and no further actions were necessary. On December 29, 2014, an unscheduled down time occurred which lasted more than 24 hours. The down time was the caused by frozen transfer lines resulting from system/discharge line upgrades. The upgrades were necessary to add three more continuous pumping wells to the chloroform pumping network. The up-sizing of the discharge line required that the old l-inch lines be excavated while the 4-inch lines were connected. During the excavation the l-inch lines, which were still connected to the existing pumping system, were exposed to the elements in the open trench. The Mill experienced below freezing temperatures for most of the week prior to December 29, 2014. The down time during construction caused six continuous pumping wells (MW-04, MW-26, TW4-04, TW4-20, TW4-22, and TW4-24) to be off (not pumping) until the completion of construction. Initial notice of this outage was given by telephone to DRC at approximately 1:00pm on Monday December 29, 2014 (within 24 hours of the discovery). As required by the O&M Plan, a 5-day written notification was also provided to DRC. The 5-day written notification is included in Tab N. The pumps were returned to service On January 9, 2015. Unless specifically noted below, no additional operational problems were observed with the well or pumping equipment during the quarter. 5.4.1 MW-04 On November 24, 2014, Mill Field Personnel noted that the discharge line from MW-04 was frozen. The frozen discharge line was likely caused by the power outage which began the previous day as noted above. Upon discovery, the discharge line was thawed and full functionality was restored within several hours of discovery. No official notifications to DRC were required as the issue was rectified within 24-hours. 26 On December 8, 2014 Mill Field Personnel noted that the heat lamp on MW-04 had burned out. No adverse affects were noted due to the nonfunctioning bulb. The bulb was immediately replaced. No official notifications to DRC were required as the issue was rectified within 24- hours. On December 22, 2014, Mill Field Personnel noted that due to intermittent power issues, the pump timer had lost its settings. The pump timer was reset immediately upon discovery. No official notifications to DRC were required as the issue was rectified within 24-hours. 5.4.2 TW 4-04 On November 24, 2014, Mill Field Personnel noted that the discharge line and the flow meter from TW4-04 were frozen. Mill Field Personnel also noted that the flow meter on TW4-04 was cracked. The frozen discharge line and flow meter was likely caused by the power outage which began the previous day as noted above. Upon discovery, the discharge line was thawed and the flow meter was replaced and full functionality was restored within several hours of discovery. No official notifications to DRC were required as the issue was rectified within 24-hours. 5.4.3 MW-26 On November 18, 2014 power was shut down to several pumping wells to upgrade the power pole transformer to accommodate more pumping wells being added to the pumping network. The power was shut down for a few hours during the upgrade. When power was restored the pumping wells were checked and it was noted that the MW-26 pump timer had lost its settings. The pump timer was reset immediately upon discovery. No official notifications to DRC were required as the issue was rectified within 24-hours. 5.4.4 TW4-25 On November 3, 2014 Mill Field Personnel noted that the TW4-25 pump had lost electrical power due to a poor connection. The well was inspected during the monthly depth check on October 29, 2014 and was fully operational at that time. The power loss happened between the monthly depth check and the weekly inspection. Some loss of pumped volume may have occurred as a result of the power loss. The power was immediately restored upon discovery. The pump timer was reset immediately upon discovery. No official notifications to DRC were required as the issue was rectified within 24-hours. On November 26, 2014, Mill Personnel notified EFRI Corporate Environmental Staff that pumping of TW4-25 had to be stopped to accommodate construction activities in the area associated with the ammonium sulfate concrete cover required under the Nitrate CAP. Pumping was stopped for several hours and no notification to DRC was necessary. On December 1, 2014, Mill Field Personnel requested cessation of pumping in TW4-25 for several days to accommodate re-routing of the discharge lines and electrical lines. The discharge and electrical lines were rerouted as a result of the ammonium sulfate concrete cover. EFRI Corporate Environmental Staff contacted DRC and requested approval for the cessation of pumping. DRC provided verbal approval and requested the incident be documented in this report. Pumping was resumed on December 4, 2014. 27 On December 8, 2014 during the weekly check, Mill Field Personnel noted that the TW4-25 pump timer had lost its settings. The pump timer was reset immediately upon discovery. No official notifications to DRC were required as the issue was rectified within 24-hours. 6.0 CORRECTIVE ACTION REPORT There are no coiTective actions required during the current monitoring period. 6.1 Assessment of Previous Quarter's Corrective Actions The third quarter nitrate report included a corrective action report to address low level nitrate contamination in the rinsate samples. Since the DIFB collected for the third quarter were non- detect, EFRI believed the nitrate present in the rinsate samples was due to laboratory contamination and did not represent actual nitrate contamination. EFRI used an alternative laboratory, CTF, during the quarter, because the Mill's usual contract laboratory, AWAL, suffered a catastrophic fire and could not accept samples. The corrective action specified in the third quarter report was to resume sending samples to A W AL as soon as their laboratory was able. The fourth quarter samples were sent to A W AL and all rinsate samples were nondetect for all analytes. As such the coiTective action is deemed closed and no further actions are required. 7.0 CONCLUSIONS AND RECOMMENDATIONS As per the CAP, the current quarter is the fifth quarter that hydraulic capture associated with nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2 was evaluated. Water level monitoring indicates that the apparent combined capture of the nitrate and chloroform pumping systems is similar to and slightly larger than to last quarter. Capture associated with nitrate pumping wells is developing and is expected to increase over time as water levels decline due to pumping and to cessation of water delivery to the northern wildlife ponds. Furthermore, the evaluation of the long term interaction between nitrate and chloroform pumping systems will require more data to be collected as part of routine monitoring. Slow development of hydraulic capture by the nitrate pumping system is consistent with and expected based on the relatively low permeability of the perched zone at the site. Definition of capture associated with the nitrate pumping system will also be influenced by the perched groundwater mound and the apparently anomalously low water level at TWN-7. CuiTent pumping is likely sufficient to eventually capture the entire nitrate plume upgradient of TW4-22 and TW4-24. Pumping during the current quarter is approximately the same as to a factor of 2.1 times greater than the estimated pre-pumping ('background') rate of perched water flow through the nitrate plume. Because the pre-pumping flow calculations likely overestimate the new 'background' conditions caused by reduced recharge from the northern wildlife ponds, and because the average plume hydraulic conductivity estimate from the low end of the calculated range is likely to be more representative of actual conditions, nitrate pumping may exceed flow through the plume by a factor greater than 2.1. 28 Fourth quarter, 2014 nitrate concentrations at many of the wells within and adjacent to the nitrate plume were within 20% of the values reported during the previous quarter, suggesting that variations are within the range typical for sampling and analytical error. Changes in concentration greater than 20% occurred in MW-26, MW-27, MW-31, TW4-10, TW4-16, TW4- 19, TW4-20, TW4-21, TW4-22, TW4-25, TWN-2, and TWN-4. The concentrations in wells MW-11, MW-25, and MW-32 remained non-detect. Of the wells showing changes in concentration greater than 20%, MW-26, TW4-19, and TW4-20 are chloroform pumping wells; and TW4-22, TW4-25 and TWN-2 are nitrate pumping wells. TW4-10 and TW4-16 are located adjacent to chloroform pumping well MW-26; TW4-21 is located adjacent to chloroform pumping well TW4-19; and TWN-4 is located between the northern wildlife ponds and nitrate pumping wells TW4-25 and TWN-2. Nitrate concentration fluctuations at pumping wells and adjacent wells likely result in part from the effects of pumping. Concentrations at TW4-21 are also influenced by its location near the eastern nitrate and northern chloroform plume boundaries. MW -31 is located in the downgradient portion of the nitrate plume and is expected to be influenced by changes in upgradient pumping at nitrate pumping wells TW4-22 and TW4-24 and chloroform pumping wells MW-26, TW4-19 and TW4-20. The nitrate concentration at TW 4-21 increased from 7.1 mg/L last quarter to 10 mg/L this quarter, bringing it again just within the nitrate plume boundary. The nitrate concentration in nitrate pumping well TW4-25 decreased from approximately 1.6 mg/L last quarter to 1.0 mg/L this quarter. The nitrate concentrations in chloroform pumping wells MW-26, TW4-19, and TW4-20 increased from approximately 0.7 mg/L, 1.6 mg/L and 4.3 mg/L, respectively, to approximately 1.1 mg/L, 4.7 mg/L, and 7.7 mg/L. The chloroform concentration at nitrate pumping well TW4-24 decreased from 76.3 f!g/L to 25.8 !!giL. The decrease at TW4-24 pushed the chloroform plume boundary back to the east of TW4-24; last quarter, a chloroform concentration increase from 62.7 f!g/L to 76.3 f!g/L moved the chloroform plume boundary to the west of TW4-24. Chloroform changes at TW4-22 and TW4-24 are likely in response to the start-up of nitrate pumping in the first quarter of 2013 and are affected by the presence of historically high chloroform concentrations at adjacent, cross-gradient well TW4-20. Increases in nitrate concentrations at wells within the nitrate plume since the last quarter have resulted in a slight expansion of the plume area. MW -27, located west of TWN-2, and TWN-18, located north of TWN-3, bound the nitrate plume to the west and north (See Figure I-1 under Tab I). In addition, the southernmost (downgradient) boundary of the plume remains between MW- 30/MW-31 and MW-5/MW-11. Nitrate concentrations at MW-5 (adjacent to MW-11) and MW- 11 have historically been low(< 1 mg/L) or non-detect for nitrate (See Table 5). MW-25, MW- 26, MW-32, TW4-16, TW4-19, TW4-20, TW4-25, TWN-1, and TWN-4 bound the nitrate plume to the east. Although short-term fluctuations have occurred, nitrate concentrations in MW-30 and MW-31 have been relatively stable, demonstrating that plume migration is minimal or absent. Nitrate in MW-30 increased from 13.8 mg/L to 16.2 mg/L and nitrate in MW-31 increased from 15.2 mg/L to 20.9 mg/L. Based on the concentration data at MW-5, MW-11, MW-30, and MW-31, the nitrate plume is under control. 29 Chloride has been relatively stable at MW-30 but is increasing at MW-31. The apparent increase in chloride and relatively stable nitrate at MW-31 suggests a natural attenuation process that is affecting nitrate but not chloride. A likely process that would degrade nitrate but leave chloride unaffected is reduction of nitrate by pyrite. The likelihood of this process in the perched zone is discussed in HGC, December 7 2012; Investigation of Pyrite in the Perched Zone, White Mesa Uranium Mill Site, Blanding, Utah. Nitrate mass removal by pumping and natural attenuation (expected to result primarily from pyrite oxidation/nitrate reduction) act to lower nitrate mass within the plume. Changes resulting from redistribution of nitrate within the plume are expected to result in both increases and decreases in concentrations at wells within the plume and therefore increases and decreases in mass estimates based on those concentrations, thus generating 'noise' in the mass estimates. Furthermore, because the sum of sampling and analytical error is typically about 20%, changes in the mass estimates from quarter to quarter of up to 20% could result from typical sampling and analytical error alone. Longer-term analyses of the mass estimates that minimize the impact of these quarter to quarter variations are expected to provide useful information on plume mass trends. Over the long term, nitrate mass estimates are expected to trend downward as a result of direct removal by pumping and through natural attenuation. As specified in the CAP, once eight quarters of data have been collected (starting with the first quarter of 2013), a regression trend line is to be applied to the quarterly mass estimates and evaluated. The trend line is then to be updated quarterly and reevaluated as additional quarters of data are collected. As the current quarter constitutes the eighth quarter as specified in the CAP, the mass estimates were plotted and a regression line fitted to the data, as shown in Figure M.1 of Tab M. The fitted line shows a decreasing trend in the mass estimates. The influence of individual wells on the mass estimates was evaluated qualitatively and quantitatively as discussed in Section 4.3. The results of the visual and quantitative analyses indicate that variations in plume mass estimates can be expected to depend primarily on variations in data from TWN-2. Wells TW4-22, TW4-24, and MW-31 (not necessarily in that order) are collectively the next most important with regard to influence on the mass estimates During the current quarter, a total of approximately 109 lb of nitrate was removed by the chloroform pumping wells and by nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN- 2. Of the 109 lb removed during the current quarter, approximately 93 lb, (or 85 % ), was removed by the nitrate pumping wells. The baseline nitrate (nitrate+nitrite as N) plume mass calculated as specified in the CAP (based on second quarter, 2010 data) was approximately 43,700 lb. The mass estimate during the current quarter was calculated as 34,370 lb which was larger than the mass estimate during the previous quarter (24,140 lb) by 10,230 lb or 42 %. This difference results from higher nitrate concentrations measured in most wells within the plume and the resulting increased areal extent this quarter compared to last quarter Nitrate concentrations outside the nitrate plume exceed 10 mg/L at a few locations: TW4-12 (16.1 mg/L), TW4-26 (12.3 mg!L), TW4-27 (28.2 mg/L), and TW4-28 (16.5 mg/L). All these 30 wells are located southeast of the nitrate plume as defined in the CAP and all are separated from the plume by wells having nitrate concentrations that are either non-detect, or, if detected, are less than 10 mg!L. Concentrations at TW4-26, TW4-27 and TW4-28 are within 20% of their concentrations during the previous quarter, while the concentration at TW4-12 increased more than 20%, from approximately 13 mg/L to 16 mg/L. From the third quarter of 2013 through the second quarter of 2014, nitrate concentrations at TW4-10 and TW4-18 exceeded 10 mg!L. Although last quarter, nitrate concentrations at both TW4-10 and TW4-18 decreased to 9.8 mg!L, both are again above 10 mg/L this quatter. Elevated nitrate concentrations at these wells are associated with the chloroform plume, and both are within the capture zone of the chloroform pumping system. Elevated nitrate at TW4-12, TW4-26, TW4-27, and TW4-28 is likely related to former cattle ranching operations at the site. Increases in both nitrate and chloride concentrations at wells near the northern wildlife ponds (for example TW4-18) were anticipated as a result of reduced dilution caused by cessation of water delivery to the nmthern wildlife ponds. However, decreasing nitrate concentrations at most wells in the vicinity of TW 4-18 over the previous three quarters after a previously increasing trend (interrupted in the first quarter of 2014) suggest that conditions in this area have stabilized. Nitrate mass removal from the perched zone was increased substantially by the start-up of nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2 during the first quarter of 2013. Continued operation of these wells is therefore recommended. Pumping these wells, regardless of any short term fluctuations in concentrations detected at the wells, helps to reduce downgradient nitrate migration by removing nitrate mass and reducing average hydraulic gradients, thereby allowing natural attenuation to be more effective. Continued operation of the nitrate pumping system is expected to eventually reduce nitrate concentrations within the plume and to further reduce or halt downgradient nitrate migration. EFRI and its consultants have raised the issues and potential effects associated with cessation of water delivery to the northern wildlife ponds in March, 2012 during discussions with DRC in March 2012 and May 2013. While past recharge from the ponds has helped limit many constituent concentrations within the chloroform and nitrate plumes by dilution, the associated groundwater mounding has increased hydraulic gradients and contributed to plume migration. Since use of the northern wildlife ponds ceased in March 2012, the reduction in recharge and decay of the associated groundwater mound was expected to increase many constituent concentrations within the plumes while reducing hydraulic gradients and rates of plume migration. The net impact of reduced wildlife pond recharge is expected to be beneficial even though it was also expected to result in temporarily higher concentrations until continued mass reduction via pumping and natural attenuation ultimately reduce concentrations. Temporary increases in nitrate concentrations are judged less important than reduced nitrate migration rates. The actual impacts of reduced recharge on concentrations and migration rates will be defined by continued monitoring. 31 8.0 ELECTRONIC DATA FILES AND FORMAT EFRI has provided to the Director an electronic copy of all laboratory results for groundwater quality monitoring conducted under the nitrate contaminant investigation during the quarter, in Comma Separated Values ("CSV") format. A copy of the transmittal e-mail is included under TabL. 32 9.0 SIGNATURE AND CERTIFICATION This document was prepared by Energy Fuels Resources (USA) Inc. on February 25, 2015. Energy Fuels Resources (USA) Inc. By: Scott Bakken Director, Permitting & Environmental Affairs 33 Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Scott Bakken Director, Permitting & Environmental Affairs Energy Fuels Resources (USA) Inc. 34 Tables Table 1 ~umtnary_ o fW liS e r de ampmgan onshtuents ~.· I Well Sample Collection Date Piezometer 01 10/8/2014 Piezometer 02 10/8/2014 Piezometer 03 10/8/2014 TWN-01 10/8/2014 TWN-02 10/8/2014 TWN-03 10/9/2014 TWN-04 10/8/2014 TWN-07 10/9/2014 TWN-07R 10/8/2014 TWN-18 10/8/2014 TW4-22 10/21/2014 TW4-24 10/2112014 TW4-25 10/21/2014 TWN-60 10/8/2014 TW4-60 12/23/2014 TWN-65 10/8/2014 Note: All wells were sampled for Nitrate and Chloride. TWN-60 is a DI Field Blank. TWN-65 is a duplicate of TWN-18. TW4-60 is the chloroform program DI Field Blank. Continuously pumped well. f h p . d or t e er10 Date of Lab Report 10/27/2014 10/27/2014 10/27/2014 10/27/2014 10/27/2014 10/27/2014 10/27/2014 10/27/2014 10/27/2014 10/27/2014 11112/2014 11112/2014 1 1112/2014 10/27/2014 11/12/2014 10/27/2014 Table 2 Nitrate Mass Removal Per Well Per Quarter MW-4 TW4-19 TW4-20 TW4-4 TW4-22 TW4-24 TW4-25 TWN-02 Quarter Totals Quarter (lbs.) MW-26 (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) 03 2010 3.2 0.3 5.8 1.7 4.7 NA NA NA NA 15.7 Q4 2010 3.8 0.4 17.3 1.4 5.1 NA NA NA NA 28.0 Q1 2011 2.9 0.2 64.5 1.4 4.3 NA NA NA NA 73.3 02 2011 3.5 0.1 15.9 2.7 4.7 NA NA NA NA 27.0 Q3 2011 3.5 0.5 3.5 3.9 5.4 NA NA NA NA 16.8 Q4 2011 3.8 0.8 6.2 2.5 6.4 NA NA NA NA 19.7 Ql 2012 3.6 0.4 0.7 5.0 6.0 NA NA NA NA 15.9 Q2 2012 3.7 0.6 3.4 2.1 5.2 NA NA NA NA 15.0 Q3 2012 3.8 0.5 3.6 2.0 4.7 NA NA NA NA 14.7 Q4 2012 3.2 0.4 5.4 1.8 4.2 NA NA NA NA 14.9 Q1 2013 2.5 0.4 14.1 1.4 3.6 8.1 43.4 7.5 14.8 95.7 Q2 2013 2.5 0.4 5.6 1.6 3.4 10.7 37.1 6.4 23.9 91.7 Q3 2013 3.0 0.4 48.4 1.4 3.8 6.3 72.8 6.9 33.4 176.5 Q42013 3.1 0.3 15.8 1.6 3.9 9.4 75.2 6.4 46.3 162.1 Q1 2014 2.7 0.4 4.1 1.2 3.6 11.2 60.4 2.3 17.2 103.1 Q2 2014 2.4 0.3 3.3 0.9 3.0 9.5 63.4 1.3 17.8 101.87 Q3 2014 2.3 0.1 4.1 0.6 3.1 8.5 56.2 1.6 16.4 92.99 Q4 2014 2.7 0.2 7.8 1.0 3.8 11.0 53.2 0.9 28.0 108.57 Well Totals (pounds) 56.3 6.9 229.6 34.4 78.9 74.7 461.6 33.4 197.8 1173.5 Table 3 Well Pumping Rates and Volumes Volume of Water Pumped Pumping Well Name During the Quarter (gals) Average Pump Rate (gpm) MW-4 63,093.0 4.39 MW-26 21,875.8 9.74 TW4-4 64,422.6 7.69 TW4-19 198,331.0 10.88 TW4-20 16,341.8 8.25 TW4-22 23,956.9 17.72 TW4-24 178.468.7 17.25 TW4-25 107,416.1 17.34 TWN-2 47,585.6 18.25 Table4 Table 4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped MW-4 MW-26 I . I 0 I Total Total Total Pumped Total Total Total Pumped Cone Cone Pumped Total Total Quarter Pumped (gal) Cone (mgll) Cone (ugll) (liters) Total (ug) (grams) (pounds) (gal) (mg/L) (ugll) (liters) Total (ug) (grams) (pounds) I Total Gallons ~ pumped for Total the quarter Total pumped Total grams/453. ' Calculations from the Concentration Concentration gallons/3. 785 Concentration ug/1000000 592 to and Data Flow Meter from the in mg/LX1000 to to conver to in ug/L X total to convert to convert to I Origination data analytical data convert to ug/L _ liters liters grams pounds Q3 2010 79859.1 4.8 4800 302266.7 1450880129 1450.9 3.20 63850.0 0.6 600 241672.3 145003350 145 0.32 Q4 2010 90042.2 5 5000 340809.7 1704048635 1704.0 3.76 60180.0 0.7 700 227781.3 159446910 159 0.35 Q12011 76247.6 4.6 4600 288597.2 1327546964 1327.5 2.93 55130.0 0.5 500 208667.1 104333525 104 0.23 Q2 2011 85849.3 4.9 4900 324939.6 1592204042 1592.2 3.51 55800.6 0.3 300 211205.3 63361581 63 0.14 Q3 2011 85327.7 4.9 4900 322965.3 1582530188 1582.5 3.49 65618.0 0.9 900 248364.1 223527717 224 0.49 Q4 2011 89735.0 5.1 5100 339647.0 1732199573 1732.2 3.82 50191.3 2 2000 189974.1 379948141 380 0.84 Q12012 90376.4 4.8 4800 342074.7 1641958435 1642.0 3.62 31440.1 1.7 1700 119000.8 202301323 202 0.45 Q2 2012 90916.5 4.9 4900 344118.8 1686181940 1686.2 3.72 26701.2 2.5 2500 101064.1 252660294 253 0.56 Q3 2012 91607.0 5 5000 346732.5 1733662475 1733.7 3.82 25246.0 2.6 2600 95556.1 248445886 248 0.55 Q4 2012 78840.0 4.8 4800 298409.4 1432365120 1432.4 3.16 30797.0 1.46 1460 116566.6 170187302 170 0.38 Q12013 62943.7 4.78 4780 238241.9 1138796304 1138.8 2.51 22650,7 2.27 2270 85732.9 194613682 195 0.43 Q2 2013 71187.3 4.22 4220 269443.9 1137053387 1137.1 2.51 25343.4 2.11 2110 95924.8 202401263 202 0.45 Q3 2013 72898.8 4.89 4890 275922.0 1349258375 1349.3 2.97 25763.0 1.98 1980 97513.0 193075651 193 0.43 Q4 2013 70340.4 5.25 5250 266238.4 1397751674 1397.8 3.08 24207.6 1.38 1380 91625.8 126443557 126 0.28 Q12014 69833.8 4.7 4700 264320.9 1242308385 1242.3 2.74 23263.1 2.12 2120 88050.8 186667767 187 0.41 Q2 2014 71934.9 4.08 4080 272273.6 1110876274 1110.9 2.45 23757.5 1.42 1420 89922.1 127689435 128 0.28 Q3 2014 74788.2 3.7 3700 283073.3 1047371347 1047.4 2.31 24062.4 0.7 700 91076.2 63753329 64 0.14 Q4 2014 63093.0 5.07 5070 238807.0 1210751515 1210.8 2.67 21875.8 0.934 934 82799.9 77335109 ___ Tl __ 0.17 ---- Totals Since Q3 2010 1415820.85 56.26 655877.7 6.88 Highlighted cells are the total for the current quarter Table 4 Table 4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped lW4-19 lW4-20 . . Total Pumped Cone 1l Cone Total Pumped Total Total Total Pumped Cone Cone Total Pumped Total Total Quarter (gal) (mg/L) · (ug/L) (liters) Total (ug) (grams) (pounds) (gal) (mg/L) (ug/L) (liters) Total (ug) (grams) (pounds) I II I I I I I Calculations I -and Data I Origination Q3 2010 116899.2 5.9 5900 442463.5 2.611E+09 2611 5.76 39098.3 5.3 5300 147987.1 784331447 784 1.73 Q4 2010 767970.5 2.7 2700 2906768.3 7.848E+09 7848 17.30 36752.5 4.6 4600 139108.2 639897778 640 1.41 Q12011 454607.9 17 17000 1720690.9 2.925E+10 29252 64.49 37187.5 4.4 4400 140754.7 619320625 619 1.37 Q2 2011 159238.9 12 12000 602719.2 7.233E+09 7233 15.95 67907.7 4.8 4800 257030.6 1.234E+09 1234 2.72 Q3 2011 141542.6 3 3000 535738.7 1.607E+09 1607 3.54 72311.2 6.5 6500 273697.9 1.779E+09 1779 3.92 Q4 2011 147647.2 5 5000 558844.7 2,794E+09 2794 6.16 72089.3 4.2 4200 272858.0 1.146E+09 1146 2.53 Q1 2012 148747.0 0.6 600 563007.4 337804437 338 0.74 76306.0 7.9 7900 288818.2 2.282E+09 2282 5.03 Q2 2012 172082.0 2.4 2400 651330.5 1.563E+09 1563 3.45 22956.4 11 11000 86890.1 955790963 956 2.11 Q3 2012 171345.0 2.5 2500 648540.8 1.621E+09 1621 3.57 22025.0 10.8 10800 83364.6 900337950 900 1.98 Q4 2012 156653.0 4.1 4100 592931.6 2.431E+09 2431 5.36 20114.0 11 11000 76131.5 837446390 837 1.85 Q1 2013 210908.0 7.99 7990 798286.8 6.378E+09 6378 14.06 18177.0 9.07 9070 68799.9 624015501 624 1.38 Q2 2013 226224.0 2.95 2950 856257.8 2.526E+09 2526 5.57 20252.4 9.76 9760 76655.3 748156060 748 1.65 Q3 2013 329460.1 17.6 17600 1247006.5 2.195E+10 21947 48.39 19731.0 8.65 8650 74681.8 645997873 646 1.42 Q4 2013 403974.0 4.7 4700 1529041.6 7.186E+09 7186 15.84 19280.2 9.64 9640 72975.6 703484369 703 1.55 Q12014 304851.0 1.62 1620 1153861.0 1.869E+09 1869 4.12 18781.6 7.56 7560 71088.4 537427971 537 1.18 Q2 2014 297660.0 1.34 1340 1126643.1 1.51E+09 1510 3.33 18462.4 5.95 5950 69880.2 415787095 416 0.92 Q3 2014 309742.0 1.6 1600 1172373.5 1.876E+09 1876 4.14 17237.9 4.3 4300 65245.5 280555441 281 0.62 Q4 2014 198331.0 4.72 4720 750682.8 3.543E+09 3543 7.81 16341.8 ~ 7670 61853.7 474417979 474 1.05 -------------- Totals Since Q3 2010 4717883.4 229.58 615012.2 34.41 Highlighted cells are the total for the current quarter Table 4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped lW4-4 lW4-22 I :1 ' Total Total Total Total Pumped Cone Cone Pumped Total Total Pumped Cone Cone Pumped Total Total Quarter (gal) (mg/L) (ug/L) (liters) Total (ug) (grams) (pounds) (gal) (mg/L) (ug/L) (liters) Total (ug) (grams) (pounds) I \ I I 1.1 . I I I II '' Calculations I and Data Origination Q3 2010 76916.8 7,30 7300.00 291130.1 2.1E+09 2125.25 4.69 NA NA NA NA NA NA NA Q4 2010 86872.1 7.10 7100.00 328810.9 2.3E+09 2334.56 5.15 NA NA NA NA NA NA NA Q12011 73360.0 7.00 7000.00 277667.6 1.9E+09 1943.67 4.29 NA NA NA NA NA NA NA Q2 2011 80334.6 7.00 7000.00 304066.5 2.1E+09 2128.47 4.69 NA NA NA NA NA NA NA Q3 2011 97535.0 6.60 6600.00 369170.0 2.4E+09 2436.52 5.37 NA NA NA NA NA NA NA Q4 2011 109043.5 7.00 7000.00 412729.6 2.9E+09 2889.11 6.37 NA NA NA NA NA NA NA Q12012 101616.8 7.10 7100.00 384619.6 2.7E+09 2730.80 6.02 NA NA NA NA NA NA NA I Q2 2012 87759.1 7.10 7100.00 332168.2 2AE+09 2358.39 5.20 NA NA NA NA NA NA NA I Q3 2012 80006,0 7.10 7100.00 302822.7 2.2E+09 2150.04 4.74 NA NA NA NA NA NA NA Q4 2012 71596.0 7.00 7000.00 270990.9 1.9E+09 1896.94 4.18 NA NA NA NA NA NA NA Q12013 58716.8 7.36 7360.00 222243.1 1.6E+09 1635.71 3.61 16677.4 58.0 58000.0 63124.0 3661189622.0 3661.2 8.07 Q2 2013 65603.4 6.30 6300.00 248308.9 1.6E+09 1564.35 3.45 25523.2 50.2 50200.0 96605.3 4849586662.4 4849.6 10.69 Q3 2013 63515.4 7.22 7220.00 240405.8 1.7E+09 1735.73 3.83 25592.9 29.7 29700.0 96869.1 2877013057.1 2877.0 6.34 Q4 2013 60233.6 7.84 7840.00 227984.2 1.8E+09 1787.40 3.94 24952.2 45.2 45200.0 94444.1 4268872280.4 4268.9 9.41 Q12014 58992.9 7.28 7280.00 223288.1 1.6E+09 1625.54 3.58 24532.0 54.6 54600.0 92853.6 5069807652.0 5069.8 11.18 Q2 2014 60235.3 5.91 5910.00 227990.6 1.3E+09 1347.42 2.97 24193.9 47.2 47200.0 91573.9 4322288622.8 4322,3 9.53 Q3 2014 69229.4 5.30 5300,00 262033.3 1.4E+09 1388.78 3.06 24610.9 41.5 41500.0 93152.3 3865818644,8 3865.8 8.52 Q4 2014 64422.6 7.02 7020.00 243839.5 1.7E+09 1711.75 3.77 23956.9 54.9 54900.0 90676.9 4978159970.9 4978.2 10.97 Totals Since Q3 2010 1365989.3 78.90 190039.4 74.72 Highlighted cells are the total for the current quarter Table 4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped TW4-24 TW4-25 i I I I Total Total Total Total ~ Pumped Cone Cone Pumped Total Total Pumped Cone Cone Pumped Total I Total Quarter (gal) (mg/L) (ug/L) (liters) I Total (ug) (grams) (pounds) (gal) (mg/L) (ug/L) (liters) Total (ug) I (grams) (pounds) .I I 1 r I 'I [I I Calculations i and Data Origination Q3 2010 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q4 2010 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q12011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q2 2011 NA NA NA NA NA NA NA NA NA NA NA NA I NA NA Q3 2011 NA NA NA NA NA NA NA NA NA NA NA NA NA I NA Q4 2011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q12012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q2 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q3 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q4 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 012013 144842.6 35.9 35900.0 548229.2 19681429751.9 19681.4 43.39 99369.9 9.0 9000.0 376115.1 3385035643.5 3385.0 7.46 Q2 2013 187509.3 23.7 23700.0 709722,7 16820428001.9 16820.4 37.08 147310.4 5.2 5240.0 557569.9 2921666087.4 I 2921.7 6.44 Q3 2013 267703.5 32.6 32600.0 1013257.7 33032202568.5 33032.2 72,82 145840.9 5.69 5690.0 552007.8 3140924419.0 3140.9 6.92 Q4 2013 260555.3 34.6 34600.0 986201.8 34122582643.3 34122.6 75 .23 126576.5 6.10 6100.0 479092.1 2922461520.3 2922.5 6.44 Q12014 229063.9 31.6 31600.0 867006.9 27397416823.4 27397.4 60.40 129979.2 2_16 2160.0 491971.3 1062657947.5 1062.7 2.34 Q2 2014 216984.1 35.0 35000.0 821284,8 28744968647.5 28745.0 63.37 124829.8 1.21 1210.0 472480.8 571701759.5 571.7 1.26 Q3 2014 213652.5 31.5 31500.0 808674.7 25473253443.8 25473.3 56.16 119663.9 1.60 1600.0 452927.9 724684578.4 724.7 1.60 Q4 2014 178468.7 35.7 35700.0 675504.0 I 24115493853.2 24115.5 53.17 107416.1 1.03 1030.0 406569.9 418767036.7 418.8 I 0.92 Totals Since Q3 2010 1698779.9 461.62 1000986.7 33.40 Highlighted cells are the total for the current quarter Table 4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped TWN-02 ... I Total I Removed Total Total by All Pumped Cone Cone Pumped Total Total Wells Quarter (gal) (mg/L) (ug/L) (liters) Total (ug) (grams) (pounds) (pounds) I Calculations and Data Origination Q3 2010 NA NA NA NA NA NA NA 15.69 I Q4 2010 NA NA NA NA NA NA NA 27.97 Q1 2011 NA NA NA NA NA NA NA 73.30 Q2 2011 NA NA NA NA NA NA NA 27.01 Q3 2011 NA NA NA NA NA NA NA 16.82 Q4 2011 NA NA NA NA NA NA NA 19.71 Q12012 NA NA NA NA NA NA NA 15,86 Q2 2012 NA NA NA NA NA NA NA 15.03 Q3 2012 NA NA NA NA NA NA NA 14.67 Q4 2012 NA NA NA NA NA NA NA 14.92 I Q12013 31009.4 57.3 57300.0 117370.6 6725334176.7 6725.3 14.83 95.73 Q2 2013 49579.3 57.7 57700.0 187657.7 10827846433.9 10827.8 23.87 91.71 Q3 2013 50036.5 80.0 80000.0 189388.2 15151052200.0 15151.1 33.40 176.53 Q4 2013 49979.9 111.0 111000.0 189173.9 20998305286.5 20998.3 46.29 162.07 Q1 2014 48320.4 42.6 42600.0 182892.7 7791229616.4 7791.2 17.18 103.14 Q2 2014 47611.9 44.7 44700.0 180211.0 8055433555.1 8055.4 17.76 101.87 Q3 2014 46927.2 42.0 42000.0 177619.5 7460016984.0 7460.0 16.45 92.99 Q4 2014 47585.6 70.6 70600.0 180111.5 12715871617.6 12715.9 28.03 108.57 Totals Since Q3 2010 371050.2 197,81 1173.58 Highlighted cells are the total for the current quarter Q2 Location 2010 MW-30 15.8 MW-31 22.5 MW-5 ND MW-11 ND ND =Not detected NS =Not Sampled Table 5 Nitrate Data Over Time for MW-30. MW-31. MW-5. and MW-11 # --Q3 Q4 Q1 Q2 Q3 Q4 Q1 Q2 Q3 Q4 2010 2010 2011 2011 2011 2011 2012 2012 2012 2012 15 16 16 17 16 16 17 16 17 18.5 21 20 21 22 21 21 21 20 21 23.6 NS 0.2 NS 0.2 NS 0.2 NS 0.1 NS ND ND ND ND ND ND ND ND ND ND ND QI Q2 Q3 Q4 QI Q2 Q3 Q4 2013 2013 2013 2013 2014 2014 2014 2014 21.4 18.8 17.6 19.5 18.4 19.4 16.8 16.2 19.3 23.8 21.7 23.9 20.6 23.1 18.9 20.9 NS ND NS 0.279 NS ND NS 0.21 ND ND ND ND ND ND ND ND TABLE 6 Slug Test Results (Using KGS Solution and Automatically Logged Data) Well K (cml.s) MW-30 1.0E-04 MW-31 7.1 E-05 TW4-22 1.3E-04 TW4-24 1.6E-04 TW4-25 5.8E-05 TWN-2 1.5E-05 TWN-3 8.6E-06 Average 1 Average2 Average 3 Average4 Notes: Average 1 = arithemetic average of all wells Average 2 =geometric average of all wells K Cft/dav) 0.28 0.20 0.36 0.45 0.16 0.042 0.024 0.22 0.15 0.32 0.31 Average 3 = arithemetic average of MW-30, MW-31, TW4-22, and TW4-24 Average 4 =geometric average of MW-30, MW-31, TW4-22, and TW4-24 cmls = centimeters per second ftlday = feet per day K = hydraulic conductivity KGS = KGS Unconfined Slug Test Solution in Aqtesolve ™. S:\Environmentai\UnWhiteMesaMiii\Required Reports\Nitrate Quarterly Report\2014 04\FiowCalcs-Tables 6-7-8: Table 6 TABLE 7 Pre-Pumping Saturated Thicknesses Depth to Depth to Water Saturated Thickness Well Brushy Basin Fourth Quarter, 2012 Above Brushy Basin (ft) (ft) (ft) TW4-22 112 53 58 TW4-24 110 55 55 Notes: ft =feet S:\Environmentai\UnWhiteMesaMill\Required Reports\Nitrate Quarterly Report\2014 04\FiowCalcs-Tables 6-7-8: Table 7 TABLE 8 Pre-Pumping Hydraulic Gradients and Flow Calculations Pathline Boundaries Path Length Head Change Hydraulic Gradient (ft) (ft) (ftlft) TW4-25 to MW-31 2060 48 0.023 TWN-2 to MW-30 2450 67 0.027 average 0.025 1 min flow (gpm) 1.31 2 max flow (gpm) 2.79 Notes: ft =feet ftlft = feet per foot gpm = gallons per minute 1 assumes width = 1 ,200 ft; saturated thickness = 56 ft; K = 0.15 ft/day; and gradient = 0.025 ft/ft 2 assumes width = 1 ,200 ft; saturated thickness = 56 ft; K = 0.32 ft/day; and gradient = 0.025 ft/ft S:\Environmentai\UnWhiteMesaMiii\Required Reports\Nitrate Quarterly Report\2014 04\FiowCalcs-Tables 6-7-8: Table 8 INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and Field Data Worksheets Tab C Kriged Current Quarter Groundwater Contour Map, Capture Zone Map, Capture Zone Details Map, and Weekly, Monthly and Quarterly Depth to Water Data Tab D Kriged Previous Quarter Groundwater Contour Map Tab E Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells Tab F Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Tab G Laboratory Analytical Reports Tab H Quality Assurance and Data Validation Tables H-1 Field Data QA/QC Evaluation H-2 Holding Time Evaluation H-3 Analytical Method Check H-4 Reporting Limit Evaluation H-5 QA/QC Evaluation for Sample Duplicates H-6 QC Control Limits for Analyses and Blanks H-7 Receipt Temperature Evaluation H-8 Rinsate Evaluation Tab I Kriged Current Quarter Isoconcentration Maps Tab J Analyte Concentration Data Over Time Tab K Concentration Trend Graphs Tab L CSV Transmittal Letter Tab M Residual Mass Estimate Analysis Figures and Tables Tab A Site Plan and Perched Well Locations White Mesa Site TW4-19 EB MW-5 • TW4-12 0 TWN-7 ~ PIEZ-1 perched chloroform or nitrate pumping well perched monitoring well temporary perched monitoring well temporary perched nitrate monitoring well Q perched piezometer TW4-32 ~ TW4-35 ¢ temporary perched monitoring well installed September, 2013 temporary perched monitoring well installed May, 2014 RUIN SPRING b seep or spring HYDRO GEO CHEM, INC. WHITE MESA SITE PLAN SHOWING LOCATIONS OF PERCHED WELLS AND PIEZOMETERS APPROVED DATE REFERENCE FIGURE H:/718000/aug 141Uwelloc0614.srf A-1 TabB Order of Sampling and Field Data Worksheets Name TWN-7 TWN-1 TWN-18 TWN-4 TWN-3 TWN-2 Duplicate of Rinsate 01 Sample Piezl Piez2 Piez 3 Nitrate Mg/L Previous Qrt. I ~ 0.9 1.7 1.8 ' 195 42.0 'f..,!IJ ~.;: 5.1 0.8 1.7 ( Nitrate Samples Oate/P1.1rp sample \D/"1/ I~ 06SS 19 IDI&II'l (),~IZ i iOJ~V l'i OZ'-11 ll0/9;/ 14 OG\"Z.~ \OJ '\il~ 07a5 '()j '6!11.\ 11..'3) 10/iSil~ {>g'-11 lOJB/1~ l''30Z tO/K/14 1'1..'-ID }D/ iY'l~ 11..50 Nitrate Order 4th Quarter 2014 Depth Total Depth 105 112.5 145 125.7 96 96 Rlnsate Samples Name Date TWN-7R 0'1'2.'1 TWN-lR TWN-18R TWN-4R TWN-3R TWN-lR Samplers: Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL See instruction FIELD DATA WORKSHEETFO GROUNDWATER Description of Sampling Event: Z.O flj Location (well name): ._I ...:.p...:.;.:::~..:.2._-....;;0_I:...._ ________ _.. Sampler Name and initials: l"i;t'ln~f" HolhJ~,:j/1] Field Sample ID I Pi~t.-D L IOO ZZOii Date and Time for Purging ._I-"-10""'/_,WIL../'-.zo_l'-'..,'-------' and Sampling (if different) l--M_;'/....:.~:---------.....J Well Purging Equip Used: IQ]pump or IT[] bailer Well Pump (if other than Bennet) 11//A ~---------------' Purging Method Used: IQ]2 casings [9]3 casings Sampling Event I Gv.art~,-l,j ;0 ;fr,.f~ Prev. Well Sampled in Sampling Event ._l_f_i_c:_-z._-_0_0 _____ __, pH Buffer 7.0 7,0 pH Buffer 4.0 LJ,O Specific Conductance ._I _l_o_o...:...o ___ ~lllMHOS/ em Well Depth(O.Olft): L-1 _o ____ _, Depth to Water Before Purging I b'3, YO Casing Volume (V) 4" Well:~_o __ --il(.653h) 3" Well:_ 0 .C.367h) Weather Cond. Ext'l Am b. Temp. ·c {prior sampling event)L-1 22 __ 0 _ ___, Time I 13 0 1 I Gal. Purged I 0 I Time I I Gal. Purged I I Conductance 1 z.t~sD I pH 1 cg,9o I Conductance I I pHI I Temp. oc I 15.3.> I Temp. oc I I Redox Potential Eh (mV) I l$0 I Redox Potential Eh (mV) I I Turbidity (NTU) I 1·:3 I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I 0 T= 2V/Q =I 0 I Number of casing volumes evacuated (if other than two) 0 If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs ._I _A_IIJ_A_L ______ ~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients B D 100ml D lJ H2S04 ~ 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250 ml D 0 No Preserv. 0 D Gross Alpl)a 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) tJ 0 Sample volume 0 tJ 0 r!J t._ hlo-r1Jc If preservative is used, specify Type and Quantity of Preservative: Final Depth ._I _£_9 _' 30 ___ _. Sample Time See instruction Comment Arr;~ DY\ ~i+c o--+-125~ --f~t~ner ~flJ (r,.r61'1 prc~c,t -+o wlleA ,Se.,..,pl~~ . ~0\Mpl('~ bo.:lea ~+ l:i>Z. \.0CA.+cc we..~ yYIO!:l.t~ c\~etr w ,-tl, o.. f~ wooJ I ;U<a P ... ..-\ic.l~~ .fldtA. -t;~ ;V1 ; -t Let.f-site tAr I~D5 L--~P:...:ie.;;;.z-....;O_l....;l:...:0_-0.;...8:...-.;;;.20.;_1_4 _ __,1Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 .. ~ Mill-Gl!lundWiltq,Discharge Permit ( Date: 06-06-lZ Rev. 7 2 -Errata GrnundWilter Monitorins Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE 1\-IESA URANIUM l\fiLL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I 4"fh Q v."r+c:r t\),1-rc;\.+c 201y . ,...J See mstruc:ti011 Sampler Name Location (well name): I P,e-z-02. and initials: I /f;w·~er t)oJI,IJ"'~ lr'H Field Sample ID p,ez-02.-IOO tS'201'i Date and Time for Purging ~...! ....lt~o'-'/g..._.'" lw2D...:.LI...&.Y ____ ___J and Sampling (if different) tJ/(1 Well Purging Equip Used: [gJ pump or IT!] bailer Well Pwnp (if other than Bennet) I fl/t,, Purging Method Used: [g]2 casings @]3 casings Sampling Event !Gv.o...d er b AJ~tc;f Prev. Well Sampled in Sampling Event 1-f'dtA -(WAJ-02 -rvJN -o-z. pH Buffer 7_0 7.0 pH Buffer4.0 L\.D Specific Conductance ..... 1 ..... I""D0'-=0~ __ __,1~MHOS! em Well Depth(O.O lft): L-1 -=0 ____ _, Depth to Water Before Purging I 35. ~ l1 Casing Volume (V) 4" WeU:~....:o::...__ __ -11(.65311) 3"WeU:_ o .(.367h) Weather Cond.. Ext'l Amb. Temp. •c (prior sampling event )IL-..:;;z;.=z:....." _ ___J Time I lZ.3'i I Gal. Purged I 0 I Time I I Gal. Purged I I Conductance I S l~ I pH I ~.'1 4 I Conduclallce I I pHI I Temp. oc I \2,lj3 I Temp. °C I I Redox Potential Eh (m V) I 23b I Redox Potential Eh (m V) l I Turbidity (NTU) I ~.s I Turbidity (NTU) l I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. °C I I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater A 1 of2 capturx· COMPA~IILE WITH/"-.,_-<>Jir-fUNCTtONHITY Min-G(oundwaleJ Discharge Permit { . Date: QD.()6-ll Rev. 7.2-Err;at;a Groundwater Monitoring Qu;aflty Assurance Pliln IQAP) VoJume ofWater Purged D gallon(s) Pwnping Rate Calculation Flow Rate (Q), in gpm. S/60= I 0 Time to evacuate two casing volumes (2V) T=2V/Q= I 0 I Number of casing volwnes evacuated (if other than two) 0 If well e\'acnated to dryness, number of gallons evacuated 0 Name of Certified Analytical Laboratory if Other Than Energy Labs ._I ..:...A,_.\J_ft:...:.=L ____ __. Sample Taken Sample Vol (indicate Filtered Preservative Added Type of SarnpJc if other than as Preservative Type VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specify) C hlor;J~ Final Depth ._I 3='=-';...;.GI_,_~ __ __, ~ Jcomment y 0 m 0 0 0 m Arr;Je~ al'\ s,·.f-c ~~..+ ,z.:;:,~ s~«~ples be~..'leJ o-+ 12'-\{) Le..\~ s :-h~. o-. t iD~3 N specified below) y D 3x40 ml 0 0 lOOm! 0 0 '250m! 0 0 250ml 0 0 1,000 .rnl 0 0 Sample volume 0 Sample Time N 0 Gil 0 0 0 EZI y HCL 0 H2S04 fll HN03 0 NoPreserv_ 0 HNOJ 0 '0 If preservative is \L<;ed, specifY Type and Quantity of Preservative: ,:J See instruction ·r -1:1\ner t:tr'IJ G--o.rr:fl pr~sevrr To coiled-~a.,vpr~..s WO\. .. h~r I.VP\..S rYJo~-H_j Cle~r N 0 0 0 0 0 B) ..__ _______ __,~IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwatl!l' A 2 of2 capturx• CDIIPATIILE WITH../'-'1-.ri;r-fUNCTIONALITV Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I '-frh G>v.o.rfer Al i1"ro-.fe zON Location (well name): L...I....~P ...... i:.:::e::..::Z.=---0=3:.......... ________ --J Sampler Name and initials: Field Sample ID Date and Time for Purging IL..._~Io;....;./_.g'"'"/....:z;...;;o;..:.IY...:........ ___ _, and Sampling (if different) Well Purging Equip Used: [Q]pump or 00 bailer Well Pump (if other than Bennet) I . See instruction Purging Method Used: [Q]2 casings (QJ3 casings Sampling Event I G~~r+crlj A)i..J.r,.ft:: Prev. Well Sampled in Sampling Event L...,_f'i_,_~_-z._-_0_~ _____ ___, pH Buffer 7.0 7.0 Specific Conductance L...l _lo_oo ____ _,l !!MHOS/ em Depth to Water Before Purging I '17. oy Weather Cond. Time 11z 9q I Gal. Purged I 0 Conductance 1 279~ I pH II!.St;: Temp. oc I !~.z~ I Redox Potential Eh (m V) I ~ I Turbidity (NTU) I :s .z: I Time I I Gal. Purged I Conductance I I pH I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater I I I I pH Buffer 4.0 !l .O Well Depth(O.Olft): l._o ____ _. Casing Volume (V) 4" Well :lt--~0=-----il ( .653h) 3"Well:_ () _(.367h) Ext'l Amb. Temp. oc (prior sampling event),_j_-z_Z._0 __ _, Time I I Gal. Purged I I Conductance I I pHI I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Time I I Gal. Purged I I Conductance I I pHI I Temp. °C I I Redox Potential Eh (mV) I I Turbidity (NTU) I I 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gprn. S/60 = I 0 Time to evacuate two ca in o volumes (2V) T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) 0 If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs ~..I_A_\J_A_L ______ ~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs 0 0 3x40 ml D 0 HCL 0 0 Nutrients ~ 0 100 ml D ~ H2S04 [::J D Heavy Metals 0 0 250m! D 0 HN03 0 0 All Other Non Radiologies 0 0 250m! 0 0 No Preserv. D D I Gross Alpl1a D 0 1,000 ml D D HN03 0 0 Other (specify) 6 0 Sample volume D 1!!1 0 ~ C h'or·,Je If preservative is used, specify Type and Quantity of Preservative: Final Depth I 5'2. SO Sample Time 1Z.50 ~,-l See instruction Comment Arr··u~a Or" ~;-tc "'t Jz. ~ -t.Fif'ler 1:)./ld. G-Arf:fl rr~~et1+ to LOlled-So.n?ples.. ~o..rvq:~l6 bilJ o..+ IZSD l.Uo..+er WC\.~ vYloStl~ Ocw-LV,·fh ~ ~;~h PH Left s.i+~ a..+ I'Z.53 Piez-03 10-08-2014 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: l l...frn Q\.l.o.r:t~r Ni+o,fe. 2.0 /'-f -See instruction Location (well name): LII"1_W_IJ_-..;;.O_l ------------J Sampler Name and initials: r:::r;..,n~( Holi;Jt!:i/IH Field Sample ID Date and Time for Purging I 10/~/Wii and Sampling (if different) AliA Well Purging Equip Used: I!I]pump or [gJ bailer Well Pump (if other than Bennet) Purging Method Used: 1}[]2 casings [QJ3 casings Sampling Event I Q"'o-rfe('~ Nifr,.fe Prev. Well Sampled in Sampling Event Ll_-r_w_tJ_-_0_7 _____ _J pH Buffer 7.0 /.0 Specific Conductance Ll ....;IO_O..;;.O ____ _.h.tMHOS/ em Depth to Water Before Purging I S 'l, '\1 Weather Cond. Time loSW1 I Gal. Purged I ~ Conductance 1 ~3Z I pH I G.9~ Temp. oc I IS.OG I Redox Potential Eh (mV) I z:so I Turbidity (NTU) I 9.b I Time lOS II I Gal. Purged I 77 Conductance I gq_:s I pH I G.Z=!q Temp. oc I JS,O~ I Redox Potential Eh (mV) I 'Z 'l:? I Turbidity (NTU) I ~.D I White Mesa Mill Field Data Worksheet for Groundwater I I I I pH Buffer 4.0 Well Depth(O.Olft): I 111..50 Casing Volume (V) 4" Well:l ~11.30 1(.653h) 3'' Well:,_ __ o __ --J. (.367h) Ext'l Amb. Temp. ·c (prior sampling event)...,l l'-4_0 __ ..... Time I D~/0 I Gal. Purged I 6' I Conductance I &9G I pH I c;,qq I Temp. oc I JS.crc I Redox Potential Eh (m V) I :Z:·z:$ I Turbidity (NTU) I ..:>,U I Time ll581 "' I Gal. Purged I ~~ I Conductance I S5Z: I pH I G/19 I Temp. °C 1 15.~0 I Redox Potential Eh (mV) I Z:d> I Turbidity (NTU) I s.z: I 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I I \.0 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casin volumes (2V) T = 2V/Q =I {;..2.3 I j o l o Name of Certified Analytical Laboratory if Other Than Energy Labs L.:l A~W_A..;.;L;__ _____ __.j Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y VOCs D 0 3x40 ml 0 Nutrients !l 0 lOOm! D Heavy Metals D D 250m! D All Other Non Radiologies 0 0 250 ml 0 Gross Alpha D D 1,000 ml D Other (specify) {] 0 Sample volume 0 C,hlori~e Final Depth I '07 I rz. Sample Time Comment Arri'.Je~ Of\ ~i+e-~+ ogoz -r;Mle( t:.1fld G-1/.,rr,"fJ pfesellf p v-r~e be.:rfl ,.+ ogo~ fv-r~ed U)ell ~~ (J._ +o+~ J Pv.r~f~ enJe~ g..ll~ ..se-..mpl~ w-er~ c.ollec.+~J ~-+ O&'lZ. Lett ~i+e rl 081~ TWN-01 10-08-2014 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N y 0 HCL 0 '[] H2S04 ~ D HN03 D 0 No Preserv. 0 D HN03 D ~ D If preservative is used, specify Type and Quantity of Preservative: See instruction .fo, fu.'~~ ~(\ ~ ~~ fVlF} ;~ ev~n+ Clf' g YYI :nv..+c~ \.001.+d" v-)01.~ C.l eGt( N 0 0 D 0 0 ~ 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan {QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I Ylh Gv..o-r+-:1"' N i +f~~ofe Z.olj [ ,. See instruction Location (well name): 1~-.-:--r_w----'--Al_-....;;o--'z.::.._ ________ ____, Sampler Name and initials: 1.-,;..lltler' Ho JJ,·J'\'1/'111 Field Sample ID Date and Time for Purging ._l _l_O..:.../-=g"'-/_Z._0-'-1"1-'--------' and Sampling (if different) 1~-._,J--'/A~-------___J Well Purging Equip Used: @]pump or [QJ bailer Well Pump (if other than Bennet) lc..orri,·,hJ0'-'5 Purging Method Used: [1[]2 casings [QJ3 casings Sampling Event I Q·->-a-rl'.:rl,j A.);+rAc Prev. Well Sampled in Sampling Event l...__l\_w_JJ_-_0_3 _____ ___, pH Buffer 7.0 /.0 pH Buffer 4.0 4,0 Specific Conductance L.l _I_OO_o ____ _JI~-tMHOS/ em Well Depth(O.Olft): 1'---'-Cfb.;;....._oo ___ _.J Depth to Water Before Purging I 27. r;;.o Casing Volume (V) 4" Well:' yq·"' ,(.653h) 3" Well: o (.367h) ~------' Weather Cond. Ext'l Amb. Temp. ·c (prior sampling event)l,_22_6 __ _. Time I l£..3 2.. I Gal. Purged I Q I Time I I Gal. Purged I I Conductance I 3~:?ag I pH I 6 • .3b I Conductance I I pHI I Temp. °C I I b. IO I Temp. oc I I Redox Potential Eh (m V) I Z~l I Redox Potential Eh (mV) I I Turbidity (NTU) I 6 .. 9 I Turbidity (NTU) I J Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH] I Temp. °C I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan {QAP) Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flow Rate Q , in .gpm. Time to evacuate two casi ng volumes (2V) S/60 = I 1~.0 T = 2V /Q = I 4 '"' I Number of casing volumes evacuated (if other than two) 0 If well evacuated to dryness, number of gallons evacuated lo Name of Certified Analytical Laboratory if Other Than Energy Labs L.I..:..A.;..;w......:...A;..;L~-----_J Sample Taken Sample Vol (indicate Filtered Type of Sample if other than as y N specified below) y N VOCs 0 0 3x40 ml 0 0 Nutrients cg D 100m! 0 ~ Heavy Metals 0 D 250 ml 0 D All Other Non Radiologies 0 D 250 ml 0 D Gross Alpha D D 1,000 ml 0 D Other (specify) 111 D Sample volume 0 IJI c,'nlor;J(. Final Depth ._I _...$!'-"6""-'''-'-J ,_/ __ __, Sample Time ._11_2_3_~ ___ __. Comment Adive~ Of\ _s;+~ ~+ IZZ7. -(,.""u MJ &c..rr:n f~"e-Sell'f +c> c.ollec.+ SOIN'tflc') c.olled·C"J "'t 1"2.33. wq,.-+~,.. we:.~ c. \e~r Let-\-s1te ~+ 1'2.35 TWN-02 10-08-2014 ID<> not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater Preservative Type Preservative Added y N HCL 0 0 H2S04 ~ 0 HN03 D D No Preserv. 0 0 HN03 D D 0 !j If preservative is used, specify Type and Quantity of Preservative: See instruction 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan {QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL See instruction FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I l{l'h GMo..d~,.. AJ,;.frAOfc: Zol'-1 Location (well name): Ll-ri~W_!V_--=03--=-----------1 Sampler Name and initials: I ""'"'u fkJJ,J,.:J Htl Field Sample ID I.__.,.._, ·_w_JJ_-....;:;0..;;;;3=--'-~-0fl--=..:;;;~;:..;:;....:.Lf-....:..._-____ _.I 1\JN-o3_10D'IZO/LJ Date and Time for Purging L.I __ IO-'-/"""ff"--/-z..;;:..o'-'1'-''i-----'-' and Sampling (if different) l 1oJ'1/Z.OI'/ Well Purging Equip Used: (I[] pump or [QJ bailer Well Pump (if other than Bennet) Purging Method Used: ~2 casings [QJ3 casings Sampling Event I .G.\~r;~..-1ul'1 .A.l,1-,.~fe Prev. Well Sampled in Sampling Event L-l-r_W_AJ_-_0_Y _____ __. pH Buffer 7.0 1.__7.:...;.'..::.0 ___ __. pH Buffer 4.0 LJ,Q Specific Conductance 1-l_lo_o_o ___ _,l~-tMHOS/ em WellDepth(O.Olft): I 4{,.00 Depth to Water Before Purging I ~/.'iS Casing Volume (V) 4" Well:,37. S8 ,(.653h) 3" Well: () (.367h) ~-~----' Weather Cond. Ext'l Amb. Temp. oc (prior sampling event),_j .:..:15'-0 __ ..~ Time I t5'152 I Gal. Purged I 9 7,bb I Time I I Gal. Purged I I Conductance I z.33o I pH I b.~z I Conductance I I pHI I Temp. °C I 111, 77) I Temp. oc I I Redox Potential Eh (m V) I :Zq3 I Redox Potential Eh (m V) I I Turbidity (NTU) I 'Z'Z I Turbidity (NTU) I I Time l o7os I Gal. Purged I 0 I Time 1 070~ I Gal. Purged IO I Conductance I 'Z-'"C71 I pH jG·KS I Conductance I ZZ8'3 I pH I b·B'J I Temp. °C 11'\,CW> I Temp. oc 119.52! I Redox Potential Eh (mV) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I Af+er White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP} Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q). in gprn. S/60 = I 1\.0 Time to evacuate two casjng volumes (2V) T = 2V /Q = I b. ~g I Number of casing volumes evacuated (if other than two) I \.25 If well evacuated to dryness, number of gallons evacuated 147. t>LI Name of Certified Analytical Laboratory if Other Than Energy Labs Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D D 3x40 ml D D HCL D D Nutrients ~ D 100 ml D ~ H2S04 ~ D Heavy Metals D D 250m! D D HN03 D D All Other Non Radiologies D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) 129 D Sample volume 0 !Kl D 1?:'] Gh \or., de If preservative is used, specify Type and Quantity of Preservative: Final Depth ._I _'1.:....~:..:...;· 6::....1..__ __ _. Sample Time '-"1 0:::::,_:7..::0c..S..___ __ _. See instruction Comment Arr;\le~ ofl s1:.t~ a..+ o"y_s -r,:11 n~<""' AnJ. &~.rrifl pre.se,-t -for f'u.rje · 'Pu..r~~ ~·M ,..+ O'IL\g Y\),r~e~ vuel\ ~~ o.... 4-o+,..\ of 1..\ Mil'lu:\~ ll.l'l~ 1..0 s~c.ondS . 'Pv-r~eJ \.U ell dc_j fl.\.~~ e. c::nJe~ ~+ D'ISZ. w~>..+cr We;..~ a... l:Hic WIW~'"\. L.d1 .~:Jh: ~--r-D"'5~ ArrlvcA 01'\ sr+C!! o..+ 070Z. ~lll'ld ~Jti"'\GA GMri, ;rcsc;;:J.. -fo c.olle.c.+ S."-""f'e.5 . Dep-tJ. -)o WtA.fer vJ~~ ~7.60 ~q.vYJplc~ bo.•.Jed o-+ L~fi .S··+e u-1-Oiog ~,iJ,Iz'l,~+ +,",e of" -:> 7 D.S I -SciMJY'"'! .. 1 TWN-03 10-08-2014 lno not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I '-JTh Q v.o.rfer AJ i frG!fc Z 0/'"1 See instruction Location (well name): IL...Ii....:......::W_.:/J~-_.:0~'1 _________ __. Sampler Name and initials: I ~...,nc:r HoJl.dea~ HJt Field Sample ID l -rwAJ-OLt_IOQ8 2.0I4 Date and Time for Purging I I0/~/2.01'1 and Sampling (if different) Well Purging Equip Used: l1[jpump or @]bailer Well Pump (if other than Bennet) Purging Method Used: 11[)2 casings @]3 casings Sampling Event I Q'-'-~rf<:rb A.J,'fr"'-t-c.. Prev. Well Sampled in Sampling Event ~..l_-n_W_N_-_18' _____ ____. pH Buffer 7.0 7.0 pH Buffer 4.0 Li.D Specific Conductance ._I _1 o_o_o ___ _.~l !!MHOS/ em Well Depth(O.Olft): J rz .. ~,76 Depth to Water Before Purging l SZ ,-:3,0 Casing Volume (V) 4" Wcll ;l Y7. C=f3 ,(.653h) 3" Well:.__o __ ___._(.367h) Weather Cond. Ext'l Amb. Temp. •c (prior sampling event)._] 1_5_0 __ _, Time I oqz.o I Gal. Purged I ~~ I Time 1 o9z1 I Gal. Purged I <l(q I Conductance I 46~ I pH I "(;,75 I Conductance 11 b~ I pHI (,.73 I Temp. oc I t9, t;& I Temp. oc I 19.10 I Redox Potential Eh (mV) I 'Z: Z9 I Redox Potential Eh (m V) I ·z:z.9 I Turbidity (NTU) I lO I Turbidity (NTU) I II I Time I o'rcz: I Gal. Purged I 110 I Time IOCIZ3 I Gal. Purged j lZI I Conductance I ~"3 I pH I b.73 I Conductance I qil I pH I 6,73 I Temp. oc I 19,f;9 I Temp. oc I )q,7"tJ I Redox Potential Eh (m V) I z:-z.:3 I Redox Potential Eh (m V) I -z.2'2: I Turbidity (NTU) I 11.3 I Turbidity (NTU) I 11.5 I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged Jz_ I gallon(s) Pumping Rate Calculation Time to evacuate two casing volumes (2V) T=2V/Q= I ~.71 I Flow Rate (Q in gpm. S/60 = I lLO Number of casing volumes evacuated (if other than two) 10 If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs AWAL Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D D 3x40 ml D D HCL D D Nutrienls e:J D 100 ml tJ rJ H2S04 rf D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologies D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) ~ 0 Sample volume 0 ~ D ~ c.nt~~~~~ If preservative is used, specify Type and Quantity of Preservative: Final Depth I 53, 'lS Sample Time See instruction Comment Arr:v~a 0"' 5-i+e: "'+ Oll09 -r:llncr ~11J Cr~>,rr.'~ rre~E'(I+ -[;. f""~-e_ "'>?d -S~1'11f''';j ev~JI'/-J: 'P lA r~ ~ b~co.f'l o..-t Dt:J 11. 'P"' ~e~ we I L -+6 r ~ ~"-fu.l of' 11 fVI i rllJ\+cs. f\Ar~e er1deJ lld1t\ So.Mf1~s w~rc coJJ~cJeJ ~-1 O'ID wc-+cr I.Vc.~ cle~r L~~+ S ."i-e 11-t 0~ ZS TWN-04 10-08-2014 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: l 411\ Q IA()('+~r 1\J 1frt>.fe 2014 [ See instruction Location (well name): .... I _=t'_vJ_IJ_-_0_1 _________ __. Sampler N arne and initials: I "1" AM,er ~o II ,'J'>\ /11+ Field Sample ID lrWfJ-07_ IOOGf'Z0/9 Date and Time for Purging I IO/g/20/Lf-and Sampling (if different) \0/~1-zo l'"l Well Purging Equip Used: (Q]pump or [gJ bailer Well Pump (if other than Bennet) Purging Method Used: 002 casings @]3 casings Sampling Event I Q\:A(Arfu-8 A) :+r ... f~ Prev. Well Sampled in Sampling Event I -rvJAJ-07 R pH Buffer 7.0 "7. 0 pH Buffer 4.0 i1.D Specific Conductance ._I _l_o_o_o ___ __,l [-tMHOS/ em Well Depth(O.Olft): I lD5.00 Depth to Water Before Purging I Kb, I Z CasingVolume(V) 4"Well:I Jz.z.g ,(.653h) 3" Well: o (.367h) L-------1 Weather Cond. Ext'l Amb. Temp. ·c (prior sampling event)._jl_3_6 __ _. Time I 07'-\3 I Gal. Purged I \(,.~25 I Time I I Gal. Purged I I Conductance I lZ~ 1 I pH 1 6.S~ I Conductance I I pHI I Temp. oc I 19.~5 I Temp. oc I I Redox Potential Eh (m V) I Z:!;;O I Redox Potential Eh (m V) I I Turbidity (NTU) I 1b.1 I Turbidity (NTU) L J Time 1 uo:::;c I Gal. Purged 13 I Time IOE>Sb I Gal. Purged lu I Conductance I l~X7 I pH I 7.3& I Conductance I Jz..rl I pH I7.;J.S I Temp. oc I lo.lJJ I Temp. oc I1S.9S I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I Af+er White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged IC>,SD gallon(s) Pumping Rate Calculation Time to evacuate two casing volumes (2V) T = 2V/Q = I '2.,2.3 I Flow Rate (Q) in gpm. s16o = I n.n Number of casing volumes evacuated (if other than two) l \.3 i If well evacuated to dryness, number of gallons evacuated 1",so Name of Certified Analytical Laboratory if Other Than Energy Labs ~...l_A_W....:A:..__L _____ __J Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients fJ 0 100 ml 0 ~ H2S04 tJ Heavy Metals 0 0 250m! 0 0 HN03 0 All Other Non Radiologi-es 0 0 250m! 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) ~ 0 Sample volume 0 ~ 0 L-h lr.mli Je If preservative is used, specify Type and Quantity of Preservative: Final Depth ._I....;;IOZ.'----7-'i ___ _. Sample Time 0G55 r,:-See instruction Comment Arr ive6 Ot'\ ~;+~ e1-+ o73'l -f,..,,c~:r MJ. G-11\r(;fl p<'c~e.nt" -for pv..~<. ?v..r~o::. bc_jq,., oo.T 07'-l<. Pv.r~ea. tAle\\ .for 0\ +a+.,J cR } Mlt'\"1+<..; 30 .S.eLDnlh. fu.r~e~ well c\~'· v.,)o.t~r ~~ YVlD~+~ C.J~c-. fv..r~e.. dldeJ. o.f C/LJ3. Left' s,i4-e oo..+ 0'1~'=- N 0 0 0 0 0 .a A(r;Jcj Df\ ~i+c o..t Db51 --r;.Mle:r eM~ &{).rr .(1 presetl+ +o (..O!I~G+ S().mpJes. D-=:p~ 1-o . \ + , 1 t '~tl·~ ,._+ -},~'~~ WiAter v.)o-S> 'l~.Z6 So.Mple~ bo..;le:a o.. Ob!:6 L~fl-sJrca. 0657. ~.SO.ft!p1:1'\j- TWN-07 10-08-2014 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP} .· _____ ~. -&·~--y----·-ATTACHMENT 1-2 ~~"'""-~ ~-~--WHITE MESA URANIUM MILL See instruction FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I \.li'h Q\A.o.f"fc r N ifr~.t~ 'Z..O/~ Location (well name): ~...I-"T'.....:....;;w__;_/J_-....;0:..../_R.;__ _______ ___. Sampler Name and initials: 1=-(o.Met" Hol/,'lJD..-;1/IH Field Sample ID Date and Time for Purging 1.__1 o_/...;:~;.;.../..:::Z'-0-'-1~.;...._------~ and Sampling (if different) !VIA '---~'---------~ Well Purging Equip Used: (IDpump or [QJ bailer Well Pump (if other than Bennet)! ...,.6-._r_v._f'_a_f:>_s ____ _, Purging Method Used: 1][12 casings [QJ3 casings Sampling Event I Q~r±vf't;1 1\) :+ro..f~ Prev. Well Sampled in Sampling Event l.__-r_vJ_JJ_-_b_0 _____ __, pH Buffer 7.0 {.0 pH Buffer 4.0 Y.o Specific Conductance ._I _I o_o_o ____ _,l ~-tMHOS/ em Well Depth(O.Olft): 1~...--0 ____ __. Depth to Water Before Purging ,_1--=o ___ _. Casing Volume (V) 4" Well:~_D ___ --l,(.653h) 3" Well:_ 0 _(.367h) Weather Cond. Ext'l Amb. Temp. oc (prior sampling event)~ll_3_11 __ _, Time I O/-zg I Gal. Purged I ~~~ r Time I I Gal. Purged I I Conductance I o .~ I pH I C,,C>S I Conductance I I pHI I Temp. °C l ls.77 I Temp. oc I I Redox Potential Eh (m V) I ">I:S I Redox Potential Eh (m V) I I Turbidity (NTU) I :z,q I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. °C I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan {QAP) Volume of Water Purged ISO gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I +s ll. D I \.0 Time to evacuate two casing volumes (2V) T = 2V/Q =I 0 I Number of casing volumes evacuated (if other than two) I~._D;;;_ __ __l If well evacuated to dryness, number of gallons evacuated ... 1 _0 ___ _. Name of Certified Analytical Laboratory if Other Than Energy Labs ._I ;;...;A'"'"W-'A..;....:;;_L _____ __. Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y VOCs 0 0 3x40 ml 0 0 HCL D Nutrients ~ 0 100 ml D ~ H2S04 ~ Heavy Metals D 0 250 ml D D HN03 D All Other Non Radiologies D 0 250m! 0 0 No Preserv, D Gross Alpha D D 1,000 ml D D HN03 D Other (specify) Ill D Sample volume 0 ~ D c... h loriJc If preservative is used, specify Type and Quantity of Preservative: Final Depth l._____.;..o ____ _, Sample Time D7z'( Comment Arrive~ on sA~ a-1-C>/12 'R',nS~Afe b~~O\"' tA-t 011 ~ 0..11~ IOO &L'Ilor"~ ot 01:. Ldf ~i+~ ~J 073S _...r' I cMlr)er p.(la &o.rrin Fresenf fO, (in~(;\+~ so (r,.lltJn.s of' SoA-p wo..-1er J<:f'lso.-+e. etJded a.+ cJ7 Z'1 TWN-07R 10-08-2014 lno not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater See instruction N 0 D D 0 D '0 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan {QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: l y-n-. Q v.GA.rf.a A1t'fr.,+i 201'7 Location (well name): ~..l _-r.L;vJ=-:....:.../J'---l.:....:~=--------------' Field Sample ID j-p.JAJ-lfL IOOf(ZOio.J Sampler Name and initials: See instruction Date and Time for Purgingj ._ _IO_)_g....;.J_z_D_I'-1 _____ _, and Sampling (if different) N'/1) ~-~-------~ Well Purging Equip Used: ~pump or [QJ bailer Well Pump (if other than Bennet) I vr 1.1\tiJ..fo ~ Purging Method Used: ~2 casings [QJ3 casings Sampling Event I Q>AM ta Cj tJ.'frAf~ Prev. Well Sampled in Sampling Event .... l_li_W_N_-_0_1 _____ ~ pH Buffer 7.0 7.0 pH Buffer 4.0 L\,0 Specific Conductance ~..1 _IO_o_o ___ ___JI !!MHOS/ em Well Depth(O.Olft): I I Y5, DO Depth to Water Before Purging I s.q .41 Casing Volume (V) 4" Well:l $5. ,g3 ,(.653h) 3" Well :_ () . (.367h) ..........,"'------~ Weather Cond. Ext'l Amb. Temp. oc (prior sampling event)._! _,_/t/..._0 __ _. Time 1 o&44 I Gal. Purged I Gf'7 I Time !ogi[5 I Gal. Purged I li2J I Conductance I 7..ri1 I pH I b. L\7 I Conductance I z.lSO I pHI b.Y7 I Temp. oc I \4 ,S\ I Temp. oc I 1~.4& I Redox Potential Eh (m V) 1 '2)4D I Redox Potential Eh (m V) I Z.2'1 I Turbidity (NTU) I IZ.. I Turbidity (NTU) I 13 I Time iD89t> I Gal. Purged I I 'Z:I I Time I D:&9 7 I Gal. Purged 1132 I Conductance I 'Z.l Oil I pH I c;, 46 I Conductance I "Z.l 8D I pH I G/-17 I Temp. °C I Ft51 I Temp. oc I lq .So I Redox Potential Eh (m V) I 2.'3~ I Redox Potential Eh (m V) I Z3i I Turbidity (NTU) I 12 I Turbidity (NTU) I ~~ I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged l3Z gallon(s) Pumping Rate Calculation Flow Rate CQ • in gpm. S/60 = I I \,0 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two ca ·ing volumes (2V) T = 2V/Q = I 10. 15 I 0 0 Name of Certified Analytical Laboratory if Other Than Energy Labs 1'--'-A,_\J....;:.._A_L _____ ___, Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs 0 D 3x40 ml 0 0 HCL 0 0 Nutrients Ill 0 lOOm! 0 [! H2S04 [11 0 Heavy Metals 0 D 250m! 0 0 HN03 0 0 All Other Non Radio"lc>_gics 0 D 250m! 0 0 No Preserv. 0 0 Gross Alpha D D 1,000 ml 0 0 HN03 0 0 Other (specify) ~ D Sample volume 0 ~ 0 IB Chlor;J.G If preservative is used, specify Type and Quantity of Preservative: Final Depth I G l , l 0 Sample Time 08~7 See instruction Comment Arrlvea bn s.1+e.. a.t og3z ~nn~r 1111J. GfH(•.TJ pr~~e.t'l+ -fCJr pv.•e~ "'.,J .s~,..,pl:a.j -evet?-J: ?ur~e.. be~t.\fl 01 f-' o&3S Pur~ed we 11 ~. fA +of., I otl2 Minv.1-~~- fur~ e. ell~ea 6\I?J 5rAwtp 1~5 co/J~c.t<::d o.+ OK~7 wc.ter ~S o.. ):·f-+le M•"Jlj vJh,f(;. Lett s;1-c ~+ 0'6'-i~ TWN-18 10-08-2014 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I LjTh Qv..o..r'fu-C..h lorOOforJVt 20 1'-1 Location (well name): ._I _IW..:....;..._L\.._--=72=-----------' Field Sample ID [ -n,.>'-l-Z2 \0Z]"20l'-i Sampler Name and initials: i •,., See instruction Date and Time for Purging ] 1 D I z 1/ -z.o la.f and Sampling (if different) .... 1 ..v_'/ A ________ _.. Well Purging Equip Used: []!]pump or @] bailer Well Pump (if other than Bennet) I C..o(rHfliAOli\S Purging Method Used: [![12 casings [QJ3 casings Sampling Event I ~~r±<!rl.v\ C.\., lo rofOrM Prev. Well Sampled in Sampling Event .... l_-r_W_'1_-_1_Y _____ __. pH Buffer 7.0 "1. c pH Buffer 4.0 Lj,_() Specific Conductance 1<--..;.lo.:....;o~o'----___ _,[f!MHOS/ em Well Depth(O.Olft): 11:).50 Depth to Water Before Purging .... 1 __;;6:..J_._z_o_...~ Casing Volume (V) 4" Well:' ~L\.\5 1(.653h) 3" W U: 0 (.367h) ,_ ___ _, Weather Cond. Ext'l Amb. Temp. oc (prior sampling event) ..... [ .1.)18.._11 __ _. Time l l~l'l.. ! Gal. Purged I 0 I Time I I Gal. Purged I I Conductance I ~'1~-z. I pH [G.9D I Conductance I I pH[ I Temp. oc I \S.SS I Temp. oc I I Redox Potential Eh (mV) I 'li9 I Redox Potential Eh (mV) I I Turbidity (NTU) I 3.0 I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (mV) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I \[>.C) Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V /Q = I ~ .1j I 0 0 Name of Certified Analytical Laboratory if Other Than Energy Labs AWAt- Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y VOCs tll 0 3x40 ml 0 rn HCL Iii Nutrients 111 D 100 ml 0 Nl H2S04 ~ Heavy Metals 0 0 250m! 0 D HN03 D All Other Non Radiologies D D 250 m1 D D No Preserv. 0 Gross Alpha D D 1,000 ml 0 D HN03 D Other (specify) Ill D Sample volume 0 l:ll D c '-'lor;ae. If preservative is used, specify Type and Quantity of Preservative: Final Depth .._I ~-Y-'--._7'-'-----' Sample Time 1313 See instruction Comment AH.;\Jc~ on ~~l~ ~J 1309 JCAM"~C'r ""J. SO\rnpl~"::> w~r-t. coJkc.i-c::~ ~1-1313 GtA.n-:(\ pf'.:-~~(1-t fo c.ollc d ~~~"~pl~s. v.=>o..tcr we.~ clear L(; \+-~ ;+ t:-17\t 13 1..5 TW4-22 10-21-2014 l.oo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 D 0 D 0 lYI 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2 -Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: "-\ih Q v..o.r-1-er C..h locoto(YYI See instruction Location (well name): .._I ---r_w_LJ-'---_2 ....:.'-1 __________ _, Sampler Name and initials: 4' ~fiYle I'" Hol!."daj /f'H Field Sample ID I -rwy -2.1-1_ 1oz 1 -z..ol'-1 Date and Time for Purging l~.-_I_O..:..../_Z.._l/;_z._o..;_r~'-1 ____ __, and Sampling (if different) I._.N_I_A ________ __, Well Purging Equip Used: IT[) pump or [QJ bailer Well Pump (if other than Bennet) I C..ot1+1n'-'oi.A S Purging Method Used: [QJ 2 casings [QJ 3 casings Sampling Event I Qv."'rf u b c.\11\oro-ForWI Prev. Well Sampled in Sampling Event ...... 1_--rw __ ~_-_z_s _____ ___. pH Buffer 7.0 1.0 pH Buffer 4.0 Specific Conductance ._I _l_o_o_o ___ __,l !J.MHOS/ em Well Depth(O.Olft): ._I _H_2_.5_0 __ __. Depth to Water Before Purging I G8'. 9?. 4" Well:l Z.S.73 ,(.653h) 3" We ll : o (.367h) L------1 Casing Volume (V) Weather Cond. Ext' IAmb. Temp. oc (prior sampling event)._! J_ll_" __ _. Time I l3b'1 I Gal. Purged [ 0 I Time I I Gal. Purged I I Conductance I 31~8 I pH I b.':)5 I Conductance I I pHj I Temp. oc I 1s .·q~ I Temp. oc I I Redox Potential Eh (m V) I lg Z I Redox Potential Eh (m V) I I Turbidity (NTU) I 1.5 I Turbidity (NTU) I J Time I I Gal. Purged I I Time [ I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp. °C I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev . 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged D gallon(s) Pumping Rate Calculation Flow Rate Q , in gpm_ S/60 = I )7,0 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two ca iri£ volumes (2V) T=2V/Q= I 3 .38 I 0 Name of Certified Analytical Laboratory if Other Than Energy Labs ._I..;..A.:...;W~A..:...;L=--------1 Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs '"tJ 0 3x40 ml 0 tJ HCL 'E D Nutrients ~ D 100 ml D ~ H2S04 f] D Heavy Metals D D 250m1 0 D HN03 0 D All Other Non Radiologies 0 0 250 rn1 0 D No Preserv. D D Gross Alpha D D 1,000 ml 0 D HN03 D D Other (specify) tJ 0 Sample volume 0 'tJ D ~ G h \o,;JG If preservative is used, specify Type and Quantity of Preservative: Final Depth I 7 :S, 3q Sample Time 1'3o.5 See instruction Comment A ( r ,''.)~a ()(\ !::. ;+e "'t 130 I -r;.t~"er ,..fiJ rJMrifl pt"c.!;.ef\+ +o c.ollec.t SP-mf)~~ co)\~Gte& o. t l:J Q.S wvJcr we..~ ~ le~r 1~01 LoY'\ fiYl \A ov..s pv.Mp 1 ~ Well TW4-24 10-21-2014 IDa not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: '-I"~" O.v.~f:fer G hlor"'ofOrfVI 'ZOio.J Sampler Name See instruction Location (well name): l'--r....:.....;.W..:...'-l...!...·-=2==S~ _________ __. and initials: 1-r;:r~,,el" Ho JJ,·;;ttll~ JrH Field Sample ID l-rw'-\-25_10Z.IZ.OI'i Date and Time for Purging I.__\ --'0/'--z.__:..:.l /_2....:0:....:1...:.~------' and Sampling (if different) ._I '-1"\/._Y._:A.;...._ _______ -' Well Purging Equip Used: []!jpump or @] bailer Well Pump (if other than Bennet) I G otl f ,nvso 1.\.S Purging Method Used: @]2 casings @]3 casings Sampling Event I Q-..\~rfc.r\.:1 C.hloro-Vorrl\ Prev. Well Sampled in Sampling Event ._l_rJ_t_A ________ -' pH Buffer 7.0 I . 0 pH Buffer 4.0 LJ.o Specific Conductance ._1_\o_o_o ___ ___JI~-tMHOS/ em Well Depth(O.Olft): IL..\~=:3w:lw' So~.-.:0;;__ _ __,~ Depth to Water Before Purging I gg :SO Casing Volume (V) 4" Well:,50.23 1(.653h) 3" Well: o (.367h) ~-----l Weather Cond. Ext'l Amb. Temp. oc (prior sampling event)'-l_,_,t8..._11 __ -' Time llZ.S\ I Gal. Purged I 0 I Time I I Gal. Purged I I Conductance I -z.~l'i I pH I b.3S I Conductance I I pH I I Temp. oc I 15,~;, I Temp. oc I I Redox Potential Eh (m V) 1 ·z~o I Redox Potential Eh (m V) I I Turbidity (NTU) I ~ I Tmbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I 171 '-1 Time to evacuate two ca ·ing volumes (2V) T=2V/Q= I ;;.en I Number of casing volumes evacuated (if other than two) l o If well evacuated to dryness, number of gallons evacuated l o Name of Certified Analytical Laboratory if Other Than Energy Labs [_I_A:....:W___:....A:....:L:__ ____ _. Type of Sample VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specify) C..hlor·,Je Final Depth ._I ....;~....;4.:..:. 1:..;.1 ___ ....~ Comment Arr-,ve~ on s;t~ "'+ L.oll~c+e~ !:!u.Mp\~.s ~+ Let+ ~i+c tA.t Sample Taken Sample Vol (indicate Filtered if other than as y N specified below) y N Iii D 3x40 ml D rn ~ D 100 ml D 1::9 D D 250m! D D D D 250 ml D D D D 1,000 ml D D ~ D Sample volume 0 1!1 Sample Time IZSZ IZ5Z cleo..r TW4-25 10-21-2014 lno not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater Preservative Type Preservative Added y N HCL rn D H2S04 ~ D HN03 D D No Preserv. D D HN03 D D D 129' If preservative is used, specify Type and Quantity of Preservative: See instruction 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2 ·Errata Groundwater Monitoring Quality Assurance Plan (QAP) OIE-'V~RGYFUELS ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I ~Th Gv..M-Fer C..l-ll oro:forNJ 20/'j See instruction Location (well name): ._1-r_'Y_Ll_-_C:D __________ -.J Sampler Name and initials: I ::::r,.flller Rbn;J~h1f Field Sample ID Date and Time for Purging I 10/2..3/z.o 14 and Sampling (if different) Well Purging Equip Used: (![]pump or [ID bailer Well Pump (if other than Bennet) Purging Method Used: @]2 casings [QJ3 casings Sampling Event Gv.o-(±erGi C,)1 1orofo rW1 Prev. Well Sampled in Sampling Event ._l_,v,_~'_fl ________ _, pH Buffer 7.0 /.0 pH Buffer 4.0 '1.0 Specific Conductance ~_I _, o_o_o ____ _JI~-tMHOS/ em Well Depth(O.Olft): ._I _o ____ __J Depth to Water Before Purging I.__D ___ ___J Casing Volume (V) 4" Well:~_O ___ -l,(.653h) 3" Well:_ 0 . (.367h) Weather Cond. Ext'l Amb. Temp. oc (prior sampling event)l._z_o_o __ _. Time I o g-z_1 I Gal. Purged !o I Time I I Gal. Purged I I Conductance I 0.7 I pH ~~-~ . I Conductance I I pHI I I :z:o. ,..., I b ·30 Temp. oc Temp. oc I I Redox Potential Eh (m V) I trr-:rJ. 1-z. 411 Redox Potential Eh (m V) I I Turbidity (NTU) I Lo I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. °C I I Temp. oc I I Redox Potential Eh (mV) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate { Q). in gpm. S/60 = I () Time to evacuate two casing volumes (2V) T= 2V/Q =I 0 I Number of casing volumes evacuated (if other than two) 0 If well evacuated to dryness, number of gallons evacuated () Name of Certified Analytical Laboratory if Other Than Energy Labs ._I _A<....J..::\.J;:;...:ft....:....;;..L _____ __. Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs ~ 0 3x40 ml D ~ HCL !ill 0 Nutrients E:Jl 0 100 ml 0 ~ H2S04 lJ 0 Heavy Metals 0 D 250 ml 0 0 HN03 0 0 All Other Non Radiologies 0 D 250 ml 0 D No Preserv. 0 D Gross Alpha D 0 1,000 ml D 0 HN03 0 D Other (specify) ~ D Sample volume D 'il 0 ~ L.-h \ on'Jc If preservative is used, specify Type and Quantity of Preservative: Final Depth 1...___.....:0~ __ _. Sample Time See instruction Comment OJ: TW4-60 10-23-2014 jo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I 1.\"11\ G\NI..rfer A);-}-r;fe ZOI '-1 -See instruction Location (well name): ._li_W_N_-_W __________ __, Sampler Name and initials: I "1;:,r\er HoI 1.J"~/1H Field Sample ID 1'1\JA>-bO_IbofS zol.., Date and Time for Purging ~o-l _l_D_l_.~_J_z.o_l't _____ ....~ and Sampling (if different) Well Purging Equip Used: [Q]pump or [QJ bailer Well Pump (if other than Bennet) Purging Method Used: [QJ2 casings [QJ3 casings Sampling Event I Q\)\o.r:fer8N •+fo--fc Prev. Well Sampled in Sampling Event ... I_N_I_A ________ _, pH Buffer 7.0 ""1.0 pH Buffer 4.0 19.0 Specific Conductance ._I _l_oo_o ____ _.l ~-tMHOS/ em Well Depth(O.Olft): 1._0 _____ _. Depth to Water Before Purging ._I --=0'-----' Casing Volume (V) 4" Well:~.....,o-----il(.653h) 3" Well:. 0 .C.367h) Weather Cond. Ext'l Amb. Temp. ·c (prior sampling eventl._l 'Z._o_-__ _. Time I 0bl.J4 I Gal. Purged I 0 I Time I I Gal. Purged I I Conductance I Q,q I pH 1 7,00 I Conductance I I pHI I Temp. oc I 'Z.I , 1'3 I Temp. oc I I Redox Potential Eh (mV) I Z :S I I Redox Potential Eh (m V) I I Turbidity (NTU) I 1' c; I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill -Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate {Q) in gpm. Time to evacuate two a ·ing volumes (2V) S/60 = I 0 T= 2V/Q =I Q I Number of casing volumes evacuated (if other than two) l o If well evacuated to dryness, number of gallons evacuated lo Name of Certified Analytical Laboratory if Other Than Energy Labs I._ ..... A ..... W.;..;..o.d~L~-------' Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D D 3x40 ml D D HCL D D Nutrients rn D lOOm! D rn H2S04 00 D Heavy Metals D D 250m! D D HN03 D D All Other Non Radiologies D D 250m! D D No Preserv. D D Gross Algha D D 1,000 ml D D HN03 D D Other (specify) ~ D Sample volume D Ei! 0 ~ C. h lor ,·J~ If preservative is used, specify Type and Quantity of Preservative: Final Depth ._I _ ____;:0:....._ __ _, Sample Time OE,'-\.5 See instruction Comment .__....;T;__WN __ -6....;0_1....;0....;-0....;8....;-2;..;0_14_-.~I Do not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 05-05-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I Ljl"h G \.\t.ti•+e.r AJ1:fr"'f<: 201'-l Location (well name): ._l _:r\-'-"",J"-'tJ....:......--'b:;.:.S=-· -----------' Field Sample ID --rwfJ-b.!)_lOOSzoJ'-1 Sampler N arne and initials: See instruction Date and Time for Purging ._l.....;.;.lo...;../.:::8-'-/....;;"Z_o...:.J-'-Y ____ ___.J and Sampling (if different) Jt// A '--~~-------~ Well Purging Equip Used: [ID pump or [Q] bailer Well Pump (if other than Bennet) Grv.I'J d:.{; ~ Purging Method Used: ~2 casings @]3 casings Sampling Event I Qv.o.l'f~r{L:j 1\),'fr.J~ Prev. Well Sampled in Sampling Event .... 1_-r_v.J_JJ_-_o_l ____ __. pH Buffer 7.0 pH Buffer 4.0 L/.D Specific Conductance ._I --'-IO_<>_D ___ __.h.tMHOS/ em Well Depth(O.Olft): I 1~5, OD Depth to Water Before Purging I S'LLJ1 Casing Volume (V) 4" Well:! 55. g:3 1(.653h) 3" Well: o (.367h) .____ ___ _, Weather Cond. Ext'l Amb. Temp. ·c (prior sampling event)._l .:...l'-1.:...1 __ ...J Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I 'Jlurbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 132 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I 11 I 0 Time to evacuate two 'a ing volumes (2V) T=2V/Q= I \D .l5 I Number of casing volumes evacuated (if other than two) 0 If well evacuated to dryness, number of gallons evacuated I o Name of Certified Analytical Laboratory if Other Than Energy Labs L-1 ~...A.~..:.W:..:....:..A..:..L.. _____ --J Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D D 3x40 ml D D HCL D D Nutrients ~ D 100 ml D IZI H2S04 elf D Heavy Metals D D 250m! D D HN03 D D All Other Non Radiologies D D 250m! D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) rB 0 Sample volume 0 o<J 0 f!l c..~)or;J-<: If preservative is used, specify Type and Quantity of Preservative: Final Depth I b I · I 0 Sample Time ._l..::.o-=~:...lti....:...1 __ _ See instruction Comment o.f -)vJAl-1~ TWN-65 10-08-2014 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 TabC Kriged Current Quarter Groundwater Contour Map, Capture Zone Map, Capture Zone Details Map, and Weekly, Monthly and Quarterly Depth to Water Data Depth to TIME WELL Water (ft.) 1250 MW-1 64.06 1029 MW-2 109.69 725 MW-3 82.71 726 MW-3A 84.65 1024 MW-5 106.10 1213 MW-11 86.20 1021 MW-12 108.21 1010 MW-14 103.15 1012 MW-15 106.05 719 MW-17 72.13 1256 MW-18 71.24 1236 MW-19 59.85 1425 MW-20 90.00 1435 MW-22 66.79 746 MW-23 115.28 1032 MW-24 113.35 1008 MW-25 75.00 916 MW-26 74.80 1224 MW-27 53.39 1034 MW-28 75.30 1029 MW-29 101.00 1206 MW-30 75.20 1208 MW-31 68.15 1211 MW-32 76.25 741 MW-33 DRY 1017 MW-34 107.71 744 MW-35 112.16 742 MW-36 110.32 1015 MW-37 110.00 NAME: Garrin Palmer, Tanner Holliday DATE: 12/17/14 TIME 927 931 929 924 932 921 934 927 926 922 919 1219 955 953 950 916 1217 1211 1305 1158 914 1306 912 1006 910 1308 936 941 956 949 944 942 958 939 947 945 952 WELL MW-4 TW4-1 TW4-2 TW4-3 TW4-4 TW4-5 TW4-6 TW4-7 TW4-8 TW4-9 TW4-10 TW4-11 TW4-12 TW4-13 TW4-14 TW4-15 TW4-16 TW4-17 TW4-18 TW4-19 TW4-20 TW4-21 TW4-22 TW4-23 TW4-24 TW4-25 TW4-26 TW4-27 TW4-28 TW4-29 TW4-30 TW4-31 TW4-32 TW4-33 TW4-34 TW4-35 TW4-36 Depth to Water (ft.) 70.25 67.86 67.65 54.83 69.80 63.26 70.07 68.45 66.45 61.15 61.05 60.25 43.90 48.86 82.36 74.80 66.02 76.25 64.17 68.40 70.14 63.22 60.40 67.03 66.86 63.78 64.54 80.13 38.28 72.44 76.40 81.31 50.91 71.00 70.35 74.15 56.82 TIME WELL 1238 PIEZ-1 1233 PIEZ-2 1231 PIEZ-3 1004 PIEZ-4 1002 PIEZ-5 1304 TWN-1 1303 TWN-2 1259 TWN-3 1229 TWN-4 TWN-5 1247 TWN-6 1253 TWN-7 TWN-8 TWN-9 TWN-10 TWN-11 TWN-12 TWN-13 1241 TWN-14 TWN-15 1244 TWN-16 TWN-17 1226 TWN-18 853 TWN-19 Depth to Water (ft.) 64.10 36.15 47.36 55.12 54.17 60.35 34.03 37.95 52.45 ABANDON 77.25 86.05 ABANDON ABANDON ABANDON ABANDON ABANDON ABANDON 61.65 ABANDON 47.45 ABANDON 59.46 53.00 TIME WELL NA DR-1 NA DR-2 1340 DR-S 1343 DR-6 738 DR-7 1353 DR-8 1349 DR-9 1347 DR-10 732 DR-11 729 DR-12 722 DR-13 1358 DR-14 1429 DR-15 NA DR-16 1401 DR-17 NA DR-18 1404 DR-19 1413 DR-20 1419 DR-21 1406 DR-22 1417 DR-23 1409 DR-24 NA DR-25 Depth to Water (ft.) ABANDON ABANDON 83.00 94.35 92.03 51.20 86.41 78.15 98.20 90.51 69.73 76.24 92.83 ABANDON 67.91 ABANDON 63.02 55.58 101.13 DRY 70.50 44.00 ABANDON @ estimated dry area MW-5 perched monitoring well showing e 5503 elevation in feet amsl TW4-12 temporary perched monitoring well 0 5580 showing elevation in feet amsl TWN-7 temporary perched nitrate monitoring ~ 5563 well showing elevation in feet amsl PIEZ-1 perched piezometer showing ~ 5591 elevation in feet amsl TW4-35 temporary perched monitoring well ~5526 installed May, 2014 showing elevation in feet amsl RUIN SPRING b 5380 seep or spring showing elevation in feet amsl HYDRO GEO CHEM,INC. KRIGED 4th QUARTER, 2014 WATER LEVELS WHITE MESA SITE DATE I REFERENCE I FIGURE H:f718000/feb15/WUUwl1214.srf I C-1 t/1.,.,_ , estimated nitrate capture zone boundary stream tubes resulting from pumping ' estimated chloroform capture zone boundary stream tubes resulting from pumping @ estimated dry area MW-5 perched monitoring well showing e 5.502 elevation in feet amsl TW4-12 0 558[1 TWN-7 A '-c;•~< y ...... ----.. ... ~ PIEZ-1 Q 559~ TW4-35 ~5526 temporary perched monitoring well showing elevation in feet amsl temporary perched nitrate monitoring well showing elevation in feet amsl perched piezometer showing elevation in feet amsl temporary perched monitoring well installed May, 2014 showing elevation in feet amsl RUIN SPRING 6 5330 seep or spring showing elevation in feet amsl HYDRO GEO CHEM,INC. H:/718000/ feb15/nitrate/Uwi1214NTcz2.srf FIGURE C-2 , .. , estimated nitrate capture zone boundary stream tubes resulting from pumping ,-,' , I MW-4 ·~~52 TW4-1 055~>1 PIEZ-2 _, 5593 TW4-35 ~S5;.lt,i estimated chloroform capture zone boundary stream tubes resulting from pumping perched monitoring well showing elevation in feet amsl temporary perched monitoring well showing elevation in teet amsl perched piezometer showing elevation in teet amsl temporary perched monitoring well installed May, 2014 showing elevation in teet amsl 5540 5535 SSJo NOTE: MW-4, MW-26, TW4-4, TW4-19, and TW4-20 are chloroform pumping wells; TW4-22. lW4•24. lW4-25. and TWN-2 HYDRO GEO CHEM,INC. GED 4th QUARTER, 2014 WATER LEVELS AND ESTIMATED CAPTURE ZONES WHITE MESA SITE H:/718000/ feb15/nitrate/Uwi1214NTcz.srf Weekly Inspection Form Time Well Depth* Comments 13LI.l MW~4 '7 1.~.1 Flow t..L 4 t~.M- J Z.35 TW4-19 6 7. L-1 2 Flow I I • :) 6-P.AA. Meter z.c~oq~"2... 7.oo 133 6 TW4-20 70.o\ Flow 8.~ t,f.tV~t- Meter 3oz.51 71 t3'-~~ TW4~4 6'l.'H Flow ~-" &P.-v\. Meter "'i "\ '6J~.3o 132.5 TWN-2 2 7. zo Flow 1 s. ~ &P,!A.. Meter 3'Ll 17~. '"iD 13:;3 TW4-22 1. '-1z. Flow 17 ~ r:P~ Meter t6"J~zb. 4o 1~2q TW4-24 q l.o-z. Flow 1l. o ~PA Meter 15'2.~3 '-to ~ IZZD TW4-25 6z . .;~ Flow 11 A ~~.ft/\.- Operational Problems (Please list well number): System Operational (If no note any problems/corrective actions) -~No {Ye_§) No /_Yes . .\ No ....... (Y"es J No eYe~ No - ('{e~ No (Yes) No ~ej No eYeS~ No (Y~o (Yes) No ~No -~No (Ya§) No Corrective Action(s) Taken (Please list well number): --------------- * Depth is measured to the nearest 0.01 feet. Weekly Inspection Form Date 10/ !3 /z6J~ Name ~tie r tloJ!;lrj , (J(-.rr•'r. R /mer System Operational (If no note T ime Well Depth* Comments any eroblems/correctlve actions} I'-!S3 MW~4 71.0 Flow l.\.3 (ve_s} No Meter SOl l 1~1,4~ (YesJ No 1'150 MW-26 ,iS, C(_5 Flow 10,0 -(YesJ No Met.er 4b 1Sl7.W (Ye~ No ~ TW4-19 ~ Flow 11.0 (YeS) No ISID 75,10 Meter z'l3'1/WJ)O ( vjS No 1~'"1/ TW4-20 71 os Flow 75,3 (Yes) No Meter 316~·oz. -(Yes~o i451 TW4-4 6q .1D Flow g,o (Y~No Meter 4~677~ :=t C ves_)Jo IL-!3'5 TWN~2 Z6.Cf0 Flow 1g u ( Yes )No Meter 3'30<62.1 q <: Yes]No 1'1 "i ~ TW4-22 (.Z L{D Flow l7.o (?"es)No Meter IE,Cl7b7,7 ?v;;J No \'1L\I TW4-24 (/t.Z~ Flow 17,3 {vei) No Meter \SSLi '2.61 -(~ No 1~'Jf TW4-25 ~\.31 Flow J!o.$ -(YeS) No Meter <1 \ \ .bbo6 ( Y9S) No Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): -----------"---------- * Depth is measured to the nearest 0.01 feet. ( ( Weekly Inspection Form Time Well Depth* I ~10 MW-4 17 4'4 Flow y_L{ t:rP..M Meter so--,q-r3.W 1.32-1.\ MW-26 11-60 Flow &f~ q,7 &B Met.er Y635~5.1D IYIS TW4-19 _6·g. 'ZO Flow ll.o &-P...-v\. Meter 2t:ft1L'1.4Loo 13_ll TW4-20 6 Cf .C> g' Flow 5$.0 6-P...-'-'\.. Meter 330.31 .0~ 133~ TW4-4 6Cj."14 Flow ~-0 &P.N\. Meter L..{-5'25 .st..J 12.SO TWN-2 Z7.'-iL Flow IS. 2.. /,.0,#\. Meter 335187 40 l3Dl TW4-22 hJ.lo Flow _U\.D k~ Meter 111 qG4 t;n I.ADT:l TW4-24 b'i.1'Z. ~. :c-Flow \1.0 &f')A.. Meter l570S2\. ~0 lt_l.n TW4-25 ~S.so Flow 'll .. 4 6-P)A Meter qzzDcp.uo Operational Problems (Please list well number): M System Operational (If no note anv problems/corrective actions) ~ No ~ No {YeS) No ~No C{_e§) No ('Yesj No \,. ~es) No {res) No ~e§) No tye~ No ---~ No ~~)No Cf'_e~ No ~No (fes) No @)No @No ~e£)No Corrective Action(s) Taken (Please list well number): ------------------- *Depth is measured to the nearest 0.01 feet. \ Weekly Inspection Form Date ,9 / z.-d 1 '-{ Name 6"'-r,. . .-Pe-.1...-.u-/ L2-~ Bel t 'd e..r System Operational (If no note T' 1me W II e 0 th* ep1 c t ommen s bl I I . ) an~ ero ems correct ve actions D'i.S.I MW-4 1'1 q~ Flow {{ --'1 _6_ f./-'\_ ~No Meter .512J~()Cf ~z... (Ye§) No O~Y'? MW-26 72. 'ZS: Flow IO .D 6P/--"\ ~,No Met,er 46'-1 5142., 36 (YeS'\No too 'i TW4-19 g-4.46 Flow I I. o &{J_.....A.."l ~ No Meter Z. 'I~ 1-':{0o. oS @J) No O't'iS TW4-20 -"]CJ.IZ.. Flow <iS-.5 6:"../V\._ {Yes~\ No Meter 3 L.l ' l q .53. (Ye~ No oq54 TW4-4 /o.'-1(( Flow ,_ (') &.,....,.._ Cfe} No Meter YS66 1q _ go lfs\ No 0'1~'-:l TWN-2 28.1.(0 Flow 1 g_6 &Pfo'\. (Yes) No Meter 3.3~2...1 ~ /0 (Yev No 0'1 Ll L TW4-22 ~1-15 Flow I ~-0 fTP..u\. (Ye§) No Meter 1_"1_30 I]. t:,() (fes ) No O'l38 TW4-24 6~-~ Flow l 6 .G G-P~ ~No Meter '-~'340'-lf.,.ct"' ~No ()C,30 TW4-25 11 4g Flow lf.3 GPM (f_e~ No Meter _5_2_U,or.; on <fe$) No Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): --------------- * Depth is measured to the nearest 0.01 feet. Monthly Depth Check Form Uo//;J..,j I ~~~~ .Rl..-.e..r Date iO/z'1/2olj Name ~Y)f\~r Time Well Depth* Time Well Depth* 0~~9 MW-4 7"' j'Z.. 1"2.'-17 TWN-1 bD.35 cq1 o TW4-1 61-'1 0 12SI TWN-2 2R 'i o lOYO TW4-2 ~g .to 12.5] TWN-3 3l.lg 1:3L1'1 TW4-3 !;5. 0'2.. 12..5~ TWN-4 .$2.. 6'2.. 1~.Sa TW4-4 6'f-l~ 13QZ. TWN-7 96.60 ...13~ TW4-5 (23.'17 12.53 TWN-18 S•l.70 oaz~ TW4-6 :Z Q• ~-rz. 't25'l MW-27 SSr]S O'f3} TW4-7 ~g.w 1.3.0 l MW-30 J5 so OiSD\ TW4-8 b]l"30 1'310 MW-31 f,8' 37 011.{5 TW4-9 ~).72. 1!::HQ TW4-28 '38'. '2$ •.?"l5GJ TW4-10 G::. \. Lj 'Z. og'Z.\ TW4-29 72.. 70 oqo4 TW4-11 f::.t.2D l~oc \ iif'ii' TW4-30 76.Ro l~os TW4-12 ~:t3 k~6: I~DZ. TW4-31 ~1.85 l~.J03 TW4-13 1-\4 I 2'i I !::Ill TW4-32 50~03 ljOS TW4-14 £$2 .2$_1; 0/5.3 TW4-33 "71 I 1"1 l31.JC. TW4-15 Z3.lg l ~56 TW4-34 7 0 .5 1 083/ TW4-16 ~6..L5 i3.2~ TW4-35 71..{.36 0117 TW4-17 7f2,.Z. ~ ljQb TW4-36 57.11 lz.~~ TW4-18 ~.gs I !j "iQ TW4-19 69:.10 i3YL{ TW4-20 70.07 OSlO TW4-21 6b.3S I :1 '17. TW4-22 Sj. 'l5 J3SZ. TW4-23 Gi.O\ 1'~~0 TW4-24 bg,'-\j t ·~w TW4-25 ~'2.1lrl 1::!!~3 TW4-26 ~4 ~59 135'1 TW4-27 S?o.ys Comments: (Please note the well number for any comments) *Depth is measured to the nearest 0.01 feet Weekly Inspection Form Date u hi'"" System Operational (If no note Time Well DeQth* Comments anv oroblems/corrective actions) 1 L.l zq MW-4 /0,2~ Flow ~ Li r~P ,AA.-(Y~ No Meter 51 gg 0 _r;_ ~4 ~ No I 4 Z.Ll MW-26 73.23 Flow ICI · 0 1..-P.M (19~-No Met.er 4 663 y L.\. \\ {Ye~ No ;....,. I Sl c) TW4-19 /6.40 Flow I 0. S &Pf-"'. &es)No Meter .3oCY~.5.57 .oo (_)'a]) No I L/?J) TW4-20 70,_'-1..~ Flow tz.-z-G_P~ (Ye~ No Meter 3S"t4S .og-~ No ~ I~>'L TW4-4 ~ 'i. 7() Flow /. 6 (rf',JV' (Yes\ No Meter 'i617ZJ.OO ['reS) No .... \35q TWN-2 2..8, 'tO Flow I !L "1 f..-P .;V\ (Yes) No Meter 3.4zoqo_6o (Yes No .... 1415 TW4-22 t.7 . qo Flow l K £') (_.,." M-_(!.e§) No Meter 1/t;~gD.IO (Ye~ No ..... 11-jiS TW4-24 6'LZO Flow 1/ 4 &P-"""-r(ej) No Meter l.!;DOtS/~ 00 (Ye§l No ' 1330 TW4-25 t;S,.so Flow ,.~ lfi.O De U\. ;Yegj No Meter '13ZSB5.tb ?Yes) No Operational Problems (Please list well number): TWY-U ......>~> £v .. "' .. cl w lav+ (lot.JCC Power-w&...S n:.: .. r+oceu(. ±o l'vmp. t.t.>(.l\. u bo..c..-k.. \-u "Pery..iicl.A.. Corrective Action(s) Taken (Please list well number): ------------------------------- * Depth is measured to the nearest O.Oi feet. Weekly Inspection Form Time We ll i3J7 MW-4 (( . .57 Flow Y .4 &FA (YeS) No Meter ~I) 2. 'Z. 7 Cj 'Z. • s s (Je~ No 1337 MW-26 ~D ·'ZD Flow q . ~ &-~'/""'--6'~j) No Met.er Y6~L\:Ji'.1~ ~No '\. 122.~ TW4-19 7~Ji2 Flow I D. o 6P/-'\ _Q'es) No Meter 3D:S2.15'-\ 00 ~ No t314 TW4-20 '11.0~ Flow g,3 ('rf' __,v\, C{~No Meter 3~ lt6£~ 17 ~No - lJ'-lO TW4-4 7D. "JO Flow {.I GPA (YeS) No Meter Ljfl 7 !..{ ljl . 7 0 (fe§) No 132Li TWN-2 1.. ~-YD Flow J ~-z.._ <1-P?'\. @~No Meter 3t46Z.ofl'. 10 _@ No I'JJC) TW4-22 ·-rz.qs Flow ~No -'' ,.., {5" \ 8'.0 &-P..I'A Meter lll6q R'. }[)_ ~eS) No ~ 13Zf TW4-24 IDI.6b Flow 1'7.0 &f',AA.. (re~· No Meter L6ZL203. 2_D f{_e§ No ' ·t~2o TW4-25 6Z.31 Flow 1 'if. o G-P..A/\. (j__eJ No Meter C1'137]3 ... go_ 6 e§J No Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): --------------- * Depth is measured to the nearest 0.01 feet. Date ~ Wll e 151 '1 MW-4 \SiD MW-26 l Lj 4~ TW4-19 tS'-10 TW4-20 !~ZU TW4-4 \45'i TWN-2 \t.../)h TW4-22 !SD3 TW4-24 11-{56 TW4-25 Weekly Inspection Form Name v~rt-IA.. D ept h* c t ommen s 65.5~ Flow 1..\.4. &PM. Meter 5'273\'\.0~ "ll.qo Flow q,o 6-P~ Met.er 47D5Z.C,.56 66.44 Flow \0.0 &P/'-"\ Meter 3osz.og6.oz_ IO-Y3 Flow K."L f:rP./V"- Meter 3&/40-If. £Cj ,[L.{ Flow l.L{ &P_A.A....._ Meter 4727_5() .9o 2.9 '?.5 Flow n g GP.I'J\ Meter 3yqq1g, ~D 61. ~1_ Flow II. I f..-P/'A Meter \l'i'l'2~.7b (;~.~5' Flow ll. y f'f"'PA Meter 163L\l..~L\.:so 61.Y3 Flow I 7.1.{ GP~ Meter tt531.\ rcl. bO ( System Operational (If no note bl I . i any: Ero ems corrective act ons} (fe§) No Cf_ei) No ~§) No ~No Cfe~ No (Ye?) No ....... {Ye§) No cV8SJ No ---(Ye~ No ~No @No d_e§)No - ("?6S) No (Ye5\No ({ev No (Y@ No ~No ~No Operational Problems (Please list well number): r.-..v v"" MW-?..E. ""-s.c..olc...J.. to b'-r-r.sc...-+. br.c.. ....... sc. J..,..~€\...,tJSI· w~rc-fay.)ce -.,.>N -bcO"=crrA ;;£€ tD Wd\:: Corrective Action(s) Taken (Please list well number): _ R. c 5s:.. + ±;.......vr l,)dt £w~&ci;"' ...... ~"'3 f"opu:l1 · * Depth is measured to the nearest 0.01 feet. Date Time Well - D'13o MW-4 D'1ZZ MW-26 I) go.{.5. TW4-19 c,~2a TW4-20 092~ TW4-4 6110'1 TWN-2 o.:li6 TW4-22 D'it:l TW4-24 C'\~~ TW4-25 Weekly Inspection Form Dept h* Comments l.l. 90 Flow 4 _ 4 h-P;.A Meter .53231 ... \ 1:.2 7~.{,~ Flow CLg bP.~ Met,er --i11641. '2..3 /'2.'1..5 Flow 11_" t7P..cA Meter :3._oss.3c16.~n 6~ . .so Flow .s • .s ~f'.AA. Meter 39o3l:,_go bq~IO Flow B.lit 6-PA Meter Ylb4'Z..4 ,Rn 4't .60 Flow j ~ .z &e.M. Meter .3530 2.._ q '1.0 bi. b3 Flow 11.6 ~(>-'""'. Meter I~ \lqo LID 61.~2 Flow Jl ('\ f-.(',).A.. Meter 11-.Y ~R l.i :.1.0 lL?_Z • '-i -z. Flow 11.1.. G-f.M.. Meter 'i613ZS. 6o System Operational (If no note anv problems/corrective actions) (YeSj No C?es) No eYe~ No c'fe~ No ('~ No (Y"e]) No ,-._ (Yes) No (YeS) No _.;:;- ~No -~No (Yes) No eYe~ No '{_e·~ No ;r9S'_)'Jo ~e~ No c...?e0 No ~ (Yes)'] No ~_)No Operational Problems (Please list well number): TwL\-y MW-y ol..'.s{..\......o...r-£t-\,.o.<, f'ou4 ti"O"'Zc,.A,, no,), M ·"·:hu-Q"'-"lt • .)'=\• 1..\ ~"Ql< ~ t!.I'~L'w_~. Corrective Action(s) Taken (Please list well number): IZ.c alA a.c.l.. flow .-.c.. +<-r """ n ... ht-y a.o6 , ....... +'-e....,-c-A £ro"t..c.-,..._ ~-~d"-"'-r-.£c \loc S * Depth is measured to the nearest 0.01 feet. . . .-. . . Monthly Depth Check Form Date I! { z..sj I '1 Name c~ ... l:i;Q; £.,._t~s.c:LI"'""'"u-1-\o/l;J~y I Time Well Depth* Time Well Depth* QS.30 MW-4 6"k~Q 1233 TWN-1 6_o.l46. l "Z5b TW4-1 {;7.cn 090'1 TWN-2 ~-!.~ -tt:> l~£j TW4-2 67.55 I 2.'-\ I TWN-3 37. '13 13QI TW4-3 55-2.3 IZ.l.lS TWN-4 5 '2-10 0'lZ.I2 TW4-4 6:'fflD 12.53 TWN-7 ~6. 0.6 1303 TW4-5 63.'1~ \Zt..\'6 TWN-18 5'r. 63 lZ.£Z TW4-6 ]".31 l250 MW-27 53-l'i 1:123 TW4-7 0..2-2 4 1259 MW-30 7.5.'-1 I 1.11] TW4-8 ~6 .5'L \3ol MW-31 6~.3~ 13Q~ TW4-9 6 . g() 122.3 TW4-28 38.~H 1'30~ TW4-10 61. Yl l:z.:B TW4-29 :zz.~]5:. j311 TW4-11 66. L.J I I Z.l.!Q TW4-30 7G,.,~Q 11:Z.l TW4-12 '-I~,QS I 'Z.41 TW4-31 ~\.f~ 12.26 TW4-13 ~9 6(2 IZ~!::l TW4-32 ,so. Z.D 1ZZ9 TW4-14 a·z. 7() I"Z.Yj TW4-33 'I-2£ 09'2.3 TW4-15 76-q''Z.. 12.3~ TW4-34 ]Qa 65. \Joq TW4-16 0.6.-1 j I'L3S TW4-35 ]4.3'4 1305 TW4-17 7(2 . .;s\ I'Z...4b TW4-36 "7-"2 '-1 123~ TW4-18 6L\~ ~I QS'SO TW4-19 111.6S a~U> TW4-20 6<i .6b IZ3& TW4-21 65.61 Q91~ TW4-22 bl~~3 12~ TW4-23 ~jl. '2.S 091~ TW4-24 ~1-12. QS!l3 TW4-25 (0, \~ \Z.i..i<is TW4-26 6'-1.1\ 1'7..30 TW4-27 '60. '-\ l Comments: (Please note the well number for any comments) *Depth is measured to the nearest 0.01 feet Weekly Inspection Form Date 11-/ z./1 L.\ System Operational (If no note Ttme W II e 0 th* eo· c t ommen s bl I an~ 2ro ems corrective actions} l2.3b MW~4 64.'-1~ Flow L-\.4 G-PJV\ ('fe§) No Meter 513~611 .ss (Ve~) No \7-27 MW~26 go.61 Flow q.R GP,....-\. ({__e~ No Met.er ~ 736 ~5 .. 5L{ (Ye§)No ..... 1300 TW4~19 6_~._yq Flow I \ • !..{ _6-P ..f-'\ ~ No Meter .38~'-J 457 0 0 d_(i?s) No 17-"Z..'-{ TW4~20 ~fi_k'() Flow 16'.L\ 6-P./V'\. c'fe~ No Meter LJos 1-.s 3{, ~·No IZ-33 TW4-4 {'i.70 Flow 7.8' &P..M @No Meter 6Z.'-l3.3o @.§) No 12. L5 TWN~2 i.j3. q & Flow I '3. 4 {,-PJV\. (Ye§) No Meter "3,51655. L{O ~No I 'Z.Z.l TW4-22 61. Ll5 Flow 17.4 GP.M.. (Ye~ No Meter 12>3393. 60 (Ve~ No _L2-I ~ TW4-24 f-.,'7.70 Flow 1&.7t_ &PA {Ye~ No Meter I{.S't,yZL.. 70 ((e§) No IZ 12... TW4~25 S?:.. 70 Flow Yes{Noj Meter q{0'1C'Jl 90 Yes~~ Operational Problems (Please list well number): Tw4-25 Corrective Action(s) Taken (Please list well number): --------------- * Depth is measured to the nearest 0.01 feet. Weekly Inspection Form Date 1'1./s/1 y Time Well Depth* I 'L3S' MW-4 7 l. '-15 1?..35 MW-26 {(.66 1310 TW4-19 6 <6, '-I z._ \ '2.3.3 TW4-20 6?,.'21 I 'Z Ll 'Z... TW4-4 6'1.8'£} IZ.IC TWN-2 3b.~2.. I "2. Z. q TW4-22 hl-55 1Zt6 TW4-24 h'~<?Z... \ 2..tl TW4-25 6g.sg Comments Flow 4. I{ GP.,.v\. Meter S L.(O'f'l '5_ 0 t1 Flow tl.t? 6-P~ Met.er L-17453£f. t2 Flow II. 0 G-PA Meter 3o6 qcn S' . {')0 Flow S-5 ~~M Meter t.ilb'17D.6C> Flow r. z. G-PA Meter 100 6Y. 3D Flow 1 «.t 6-P..v\-. Meter 3b0 472-~0 Flow 1&-0 t;.f,M.._ Meter 1g-L.J ~~? ~{) Flow 17 . 8'" f... PM Meter 1665K4 Ll .so Flow 1"1.1.... &PA Meter _g7 o c;;\41 oo System Operational (If no note anv problems/corrective actions) {"{eS) No de]> No ' rf_es) No ~((a"§) No ' lf':esj No ~No (vev No {Ye~No cY_~S) No ~No (Yes) No ?(95) No (_ve.£) No ~No ...____ _(Y~s~o ~No &.BS:> No _d_e]_ No Operational Problems (Please list well number): TI~M<LC o"" T~.V"l-'2..5' \o.,t ~¢.1-~;"'fi! ptvc. +o bc.i~ oC\t. Hu...!: \4~ bvlb we,.....+-o .. rt oAr ,.-,..ua.t ,1::'\\..)-4 Corrective Action(s) Taken (Please list well number): f2.e..sM: \-i"""cr o-=ca....>L\ -'2..5 (.)., .... ~ tA~+c./t.~. IZ.c.Q\"-'-<.4'> b...,\lo o""'-MW-\..>{, * Depth is measured to the nearest D.D1 feet. Weekly Inspection Form Time Well Depth*-Comments 14.:3'-{ MW-4 /3,1~ Flow 4 ..... l &P#\ Meter .51.1~1.\~5. gi 1 '-1 (_{, MW-26 f,Cj.]O Flow ct.o G-t~ Met.er 416'1 OS. tl ~ TW4-19 7.5 'qz_ Flow 11-0 &P..,...,.._ Meter 3DIY3,Z.€;.CO j!.-lJ'o TW4-20 /,'?, zo Flow g_ z c;. I' ,IV\. Meter '"iZ'iD~ 5 g L438 TW4-4 6 c; g{ Flow ~-o GP..v\ Meter 161..\ID~tto l '4 11 TWN-2 30.(0 Flow \<d. z.. &b-"1 I Meter 36'-1091.30 I ~::P-6 TW4-22 hCf.3Z. Flow I I< l & P_/VI. Meter 1Bh'f6 (, 3o I Yl."Z. TW4-24 6'7. L{ 0 Flow 1 ..., _ e &P.AA.. Meter 16770 1'Lbo \'-\ID TW4-25 61L40 Flow l7.Y GPM Meter qf(tc.6o,oo Operational Problems (Please list well number): System Operational (It no note anv problems/corrective actions} _6ej) No (Yes) No _('165 ) No (Jes_J No ({:e~) No d"e§) No (~No (~No (Y'es_., No cY~s> No C{_~ No (eS) No cY_e_§ No <le]) No tre§_ No ~No @_§) No CieD No Corrective Action(s) Taken (Please list well number): --------------- ~ Depth is measured to the nearest 0.01 feet. ( Weekly Inspection Form Date 1 2 / ~ z.l , .. 1 Time Well -Depth* Comments \30.> MW-4 {;£..\, g'o Flow 4 . '-\ Gf'.;VL Meter 5'-i ~5 Z.l. Y5 I :3o z. MW-26 /1.15 Flow lo. c ~./-"\ Met.er Llf &.SC> \ -~2 134~ TW4~i9 t: J/1. I y Flow l \'C) &(JA Meter ~c.n<t543.oo \3\6 TW4-20 ~~ 1() Flow I .L.{ 6-~_,y Meter '-\ Y'2..5 f(~ 2.. q \3\0 TW4-4 ~'1.'lo Flow 1-6 G-f' ...-v\. Meter -z,o.t'\2 '?o l'l5l TWN-2 3\. ~0 Flow J/ # 2. G-I'M Meter 3bttL\\.IO 17.5~-TW4-22 6o.73 Flow !1.5 &P,AA.... Meter j ~~72l 30 12..5.£ TW4-24 6S,3o Flow 1/.6 f,-PA. Meter I (:.81 ~ ~.S .. 3 o IZ.4 ~ TW4-25 5t..l .7q Flow \b.g (;,.P,.AA.. Meter 9 ~ 12..S3_. bD Operational Problems (Please list well number): System Operational (If no note anv problems/corrective actions) ~ No &a& No (leS)No {rev No ...._ (Yes "No (Ye.§l No )feS No ~.No - (YeS\ No (f6f) No ~ 6'_e~ No ~ No ~No (')'eS) No {fes) No @.5) No _ ... (Ye) No tfe~ No Corrective Action(s) Taken (Please list well number): rz'-= p t-~..6 f:h"""-e.. .J.... c...J d l C<!.t -f-., -"-cSJ ,. Depth is measured to the nearest 0.01 feet. ( Weekly Inspection Form Time Well Depth* Comments I'"Z.o_7_ MW-4 AI..{. ~o Flow Meter S52.582. -"1'1 I "2.6 '1. MW-26 ;;~. rD Flow -- Met.er 4/li4 'in .56 11..\ol TW4-19 6 t.f. 7 z. Flow I\. I) 6-f.l"-"-- Meter .30 h'\.1 u-z _ o o tZOO TW4-20 r:7.cc~\ Flow 7 ., &!'l~ Meter 45~o;. o3 \'2.0~ TW4-4 6~-0Z.. Flow --- Meter 2.45'Z..4 b() II t4 i TWN-2 3'1 .8l Flow 1 ~ ~ &"J\..\. Meter 311DSo '2..0 1156 TW4-22 SR.~D Flow i ~.o &f.M Meter 1 'roo 2-'1 '-{D 11.5"Z. TW4-24 (;l, ~'1 Flow ,,_, G·I'AA- Meter Jl'1CJ:T/ q_ 'lo I 1&-1 Y. TW4-25 ,(Z./ Ll Flow n. z. 61~ Meter 1 ooo'1 Sl6 lt'J Operational Problems (Please list well number): !<...,e-s '*Cs.. £caz k'>- System Operational (If no note any problems/corrective actions) Yes{NO\ Yes~ - Yes (No) Yes(KfO) -_r-... (Y~ No 6§) No (Y'es\No (Yes J No Yes @o) Yes Ng) ~ (ie~ No ~)No ~No .~No ~ rve5'\No (reS) No (Ye§) No <Yes') No Corrective Action(s) Taken (Please list well number): llu. • ..\-l... I k)<-ll&S:·\ 5 ao k., w!+L.... fL... \ lrob!c.. Q..~ l-..H.l\.s ••. n'll be.. Stp.r-te-J.. viA'-"-..J~\l,S 7e..tc... e-o~-"'--(..ccfGq{ -f-o """C.~rsl .,A_,~d.-.e.r-c.S<:.. l""- • Depth is measured to the nearest 0.01 feet. TabD Kriged Previous Quarter Groundwater Contour Map @ estimated dry area MW·S perched monitoring well showing .5503 elevation in feet amsl TW4·12 temporary perched monitoring well 0 !:1"580 showing elevation in feet amsl TWN-7 temporary perched nitrate monitoring ~ 5563 well showing elevation in feet amsl PIEZ·1 perched piezometer showing Q 5592 elevation in feet amsl TW4-35 temporary. perched monitoring well ~5526 Installed May, 201 4 showing elev~tlon In fe~t amsl RUIN SPRING 0 5380 seep or spring showing elevation In feet amsl HYDRO GEO CHEM,INC. KRIGED 3rd QUARTER, 2014 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H:l718000/nov14/Uwl0914.srf I D-1 TabE Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells -c. E -.c ~ -Q) E i= :to.. Q) > 0 -~ Q) ...J :to.. Q) -~ ,.. I z ~ 9~/0~/90 £~/v~/80 G~H0/"170 0 ~/8 ~~~ ~ 60/90/LO 80/GG/GO q 0 0 0 q 0 C\J q 0 C') 0 0 """ l ~ ~ • 0 0 LO • 0 0 <D 0 0 ,...... -c. E -.c = -Cl) E i= a.. Cl) > 0 'ii > Cl) ..J a.. Cl) -~ N I z ~ 9~/0 ~/90 £ ~/v ~/80 uno1vo 0 ~/8 ~~~ ~ 60!90/LO 80/~~/~0 . - 0 0 q lO 0 0 ,.... { ~ ~ ~~ ~~ q 0 C\J ... r--- " " + ~ / q lO C\J q 0 C') [>. 0 0 "<t 9~/0~/90 -a. E £ ~~v~/80 -.c ....: --(1) E i= ... (1) > 0 c~/~0/170 Gi > (1) ...I ... (1) -~ M I 0~/8 ~H ~ z ~ 60/90/LO 80/cc/cO - 0 0 0 Lri C! 0 ...... C! lO ,.... 0 0 (\J 0 Lri (\J ~ ~ ~ ~ ~ i !/ 0 0 (t') ~ 1 ~ v ~ • 0 0 '<t C! lO '<t -Q. E :a =:: -Q) E i= .... Q) > 0 a; > Q) ...J .... Q) -~ ~ I z s: 1- 9~/0~/90 8 ~/17~/80 G~/~0/170 0 ~/8~H ~ 60/90/LO 80/GG/GO - - 0 0 0 0 ,..- f • ~ \ • v i q 0 L() 0 0 co -Q. E £~/v~;so jS ...; --C1) E i= :I.. C1) > 0 G~/~0/170 'CD > C1) .J :I.. C1) -~ CD I 0~/8~H ~ z ~ 60!90/LO (£) (X) 0 .... (£) 9' 0 Depth Below Measuring Point (ft.) (£) ~ 0 (£) F\:) 0 (£) 0 0 '\ 4( ~ ~ (X) (X) 0 ~\ ; (X) (]) 0 \ \ - (X) ~ 0 - 02/22/08 07/06/09 11/18/10 04/01/12 08/14/13 12/27/14 05/10/16 -1 :e z I ....... ~ .... (1) ""' r-(1) < (1) 0 < (1) ""' ::1 3 (1) -== 0"' -3 "'C - 9~/0~/90 ', -c. E ~ 1i = -Q) £ ~~v~/80 E . i= 1.. Q) > 0 -Q) > Q) -1 1.. Q) -U/~0/vO ~ '11:1' ,_ I z ~ 0~/8~/~ ~ 60!90/LO r---r---p:. ~ K ~ ~ lr I~ \ ~ [/ ~ ..__ --. C\1 cY:i co co cY:i co -c. E -.c . = -cu E i= .... cu > 0 cu > cu ..J .... cu -~ tO ,.... I z 3: 1- 9 ~/0 ~/SO ,------r-----,--------r------r----r-----, 8 ~~v~;so c~HO/vO - 60/90/LO .,._----1-----+-------1-----1----t----1 L() c.ci '<t L() o) '<t -Q. E -.c ~ -Q) E i= ... Q) > 0 -~ Q) ...J ... Q) -~ co ~ I z 3l: ~ 9~/0~/SO v~/LG/U 8 ~/v~/BO G~notvo . 60/90/LO 0 0 0 0 T'"'" 0 0 C\1 0 0 (') ~ ., ~ ~ F=: -----~ ..-:::: .._______,~ ~ ~~ ..::::::: -----. 0 0 "<t 0 0 I{) 0 0 <!) 0 0 ,..._ -c. E :a ::: -CIJ £~/v~!BO E i= lo.. ~ 0 Q) > CIJ ..J lo.. CIJ -C:~H0/170 ~ 0') ,.. I z s: 1- -c. E -.c = -G) E t= ... ~ 0 ~ G) ..J ... G) -~ 0 C") I 3: ~ 9 ~10 ~/SO ,..-----,-----.------,..-----.-----.-------. 17~/LG/G~ 8~/17~/BO G~/~0/170 0~/B~/~ ~ · 60/90/LO BO/GG/GO 90/0~/0~ SO/BG/90 +----+------+-----1-----t-----+------1 0 c) co (X) 1\) 0 (X) 0 0 ' Depth Below Measuring Point (ft.) -....! (X) 0 -....! (j) 0 ---...... ..--- -....! ~ 0 -....! 1\) 0 ' ----~ -....! 0 0 ~ ~ " \ ~ ~ ~ (j) (X) 0 ~ ~ i\ ; 1 (j) (j) 0 . - 05/28/05 10/10/06 02/22/08 07/06/09 11/18/10 04/01/12 08/14/13 12/27/14 05/10/16 s: ~ w ..... ~ -CD ., r-CD < !. 0 ~ ., ::f 3 CD -:= 2: 3 "0 - TabF Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Water Levels and Data over Time White Mesa Mill-Well TWN-1 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,646.96 5,648.09 1.13 112.5 5,600.38 02/06/09 47.71 46.58 5,599.99 07/21/09 48.10 46.97 5,600.26 09/21/09 47.83 46.70 5,601.10 10/28/09 46.99 45.86 5,602.59 12/14/09 45.50 44.37 5,600.55 03/11/10 47.54 46.41 5,600.66 05/11/10 47.43 46.30 5,599.18 09/29/10 48.91 47.78 5,598.92 12/21/10 49.17 48.04 5,598.29 02/28/11 49.80 48.67 5,597.80 06/21111 50.29 49.16 5,597.32 09/20/11 50.77 49.64 5,597.15 12/21/11 50.94 49.81 5,596.54 03/27/12 51.55 50.42 5,596.52 06/28/12 51.57 50.44 5,595.03 09/27/12 53.06 51.93 5,596.62 12/28/12 51.47 50.34 5,593.54 03/28/13 54.55 53.42 5,592.38 06/27/13 55.71 54.58 5,591 .65 09/27/13 56.44 55.31 5,590.34 12/20/13 57.75 56.62 5,590.03 03/27/14 58.06 56.93 5,589.09 06/25/14 59.00 57.87 5,588.15 09/25/14 59.94 58.81 5,587.74 12/17/14 60.35 59.22 Water Levels and Data over Time White Mesa Mill-Well TWN-2 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) lonitol"ing (blw.MP) (blw.LSD) Well 5,625.75 5,626.69 0.94 95 5,611.37 02/06/09 15.32 14.38 5,610.63 07/21109 16.06 15.12 5,609.73 09/21/09 16.96 16.02 5,607.08 11/02/09 19.61 18.67 5,606.57 12/14/09 20.12 19.18 5,612.45 03/11/10 14.24 13.30 5,612.78 05111110 13.91 12.97 5,611.37 09/29/10 15.32 14.38 5,610.24 12/21/10 16.45 15.51 5,610.64 02/28111 16.05 15.11 5,609.78 06/21/11 16.91 15.97 5609.79 09/20/11 16.90 15.96 5609.72 12/21111 16.97 16.03 5,605.69 03/27/12 21.00 20.06 5,605.67 06/28/12 21.02 20.08 5,603.03 09/27112 23.66 22.72 5,605.76 12/28112 20.93 19.99 5,598.28 03/28113 28.41 27.47 5,594.32 06/27113 32.37 31.43 5,594.38 09/27/13 32.31 31.37 5,594.68 12/20113 32.01 31.07 5,597.79 03/27/14 28.90 27.96 5,595.80 06/25/14 30.89 29.95 5,587.67 09/25114 39.02 38.08 5,592.66 12/17114 34.03 33.09 Water Levels and Data over Time White Mesa Mill -Well TWN -3 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,633.64 5,634.50 0.86 110 5,603.77 02/06/09 30.73 29.87 5,602.37 07/21/09 32.13 31.27 5,602.34 09/21109 32.16 31.30 5,602.60 10/28/09 31.90 31.04 5,603.12 12/14/09 31 .38 30.52 5,602.90 03111110 31.60 30.74 5,603.23 05111110 31.27 30.41 5,602.86 09/29/10 31.64 30.78 5,603.35 12/21110 31.15 30.29 5,602.89 02/28/11 31.61 30.75 5,602.75 06/21111 31.75 30.89 5,602.40 09/20/11 32.10 31.24 5,602.40 12/21111 32.10 31.24 5,601.70 03/27112 32.80 31.94 5,601.67 06/28112 32.83 31.97 5,600.50 09/27/12 34.00 33.14 5,601.74 12/28112 32.76 31.90 5,598.60 03/28113 35.90 35.04 5,597.18 06/27/13 37.32 36.46 5,597.36 09/27113 37.14 36.28 5,597.60 12/20/13 36.90 36.04 5,598.00 03/27/14 36.50 35.64 5,596.34 06/25/14 38.16 37.30 5,596.30 09/25/14 38.20 37.34 5,596.55 12117114 37.95 37.09 Water Levels and Data over Time White Mesa Mill-Well TWN-4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,641.04 5.64 1.87 0.83 136 5 601.47 02/06/09 40.4 0 39.57 5,604.26 07/21/09 37.61 36.78 5,605.02 09/21/09 36.85 36.02 5,605.87 10/28/09 36.00 35.17 5,605.81 12114/09 36.06 35.23 5,605.31 03/11110 36.56 35.73 5,605.36 05111110 36.51 35.68 5,604.59 09/29/10 37.28 36.45 5,604.42 12/21110 37.45 36.62 5,603.69 02/28/11 38.18 37.35 5,603.36 06/21111 38.51 37.68 5,602.82 09/20111 39.05 38.22 5,602.79 12/21111 39.08 38.25 5,600.82 03/27112 41.05 40.22 5,600.84 06/28/12 41.03 40.20 5,598.47 09/27112 43.40 42.57 5,600.86 12/28/12 41.01 40.18 5,595.57 03/28113 46.30 45.47 5,594.12 06/27/13 47.75 46.92 5,593.33 09/27113 48.54 47.71 5,591.92 12/20113 49.95 49.12 5,591.85 03/27114 50.02 49.19 5,590.49 06/25/14 51.38 50.55 5,589.64 09/25114 52.23 51.40 5,589.42 12/17/14 52.45 51.62 Water Levels and Data over Time White Mesa Mill-Well TWN-6 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,663.03 5,664.94 1.91 135 5,589.52 08/25/09 75.42 73.51 5,589.46 09/22/09 75.48 73.57 5,589.61 11/03/09 75.33 73.42 5,589.92 12114/09 75.02 73.11 5,590.24 03111/10 74.70 72.79 5,590.40 05/11110 74.54 72.63 5,590.24 09/29110 74.70 72.79 5,590.49 12/21110 74.45 72.54 5,590.16 02/28111 74.78 72.87 5,590.44 06/21/11 74.50 72.59 5,590.35 09/20111 74.59 72.68 5,590.67 12/2111] 74.27 72.36 5,590.34 03/27112 74.60 72.69 5,590.32 06/28112 74.62 72.71 5,589.77 09/27112 75.17 73.26 5,589.67 12/28112 75.27 73.36 5,589.45 03/28/13 75.49 73.58 5,589.01 06/27113 75.93 74.02 5,588.99 09/27113 75.95 74.04 5,588.15 12/20113 76.79 74.88 5,588.50 03/27114 76.44 74.53 5,588.03 06/25/14 76.91 75 .00 5,587.74 09/25/14 77.20 75.29 5,587.69 12117114 77.25 75.34 Water Levels and Data over Time White Mesa Mill -Well TWN-7 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,647.39 5,649.26 1.87 120 5,552.56 08/25/09 96.70 94.83 5,558.34 09/21/09 90.92 89.05 5,558.82 11/10/09 90.44 88 .57 5,558.96 12114/09 90.30 88.43 5,559.54 03111110 89.72 87.85 5,559.60 05/11/10 89.66 87.79 5,559.83 09/29/10 89.43 87.56 5,559.00 12/21/10 90.26 88.39 5,559.68 02/28/11 89.58 87.71 5,560.43 06/21/11 88.83 86.96 5,560.46 09/20/11 88 .80 86.93 5,560.78 12/21111 88.48 86.61 5,560.92 03/27112 88.34 86.47 5,560.87 06/28/12 88.39 86.52 5,561.40 09/27/12 87.86 85.99 5,561.50 12/28/12 87.76 85.89 5,562.01 03/28/13 87.25 85.38 5,562.21 06/27/13 87.05 85.18 5,562.41 09/27113 86.85 84.98 5,562.23 12/20/13 87.03 85.16 5,562.85 03/27/14 86.41 84.54 5,562.95 06/25114 86.31 84.44 5,563.06 09/25/14 86.20 84.33 5,563.21 12117/14 86.05 84.18 Water Levels and Data over Time White Mesa Mill-Well TWN-14 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5. >47.80 5,649.53 1.73 135 5,586.18 11/04/09 63.35 61.62 5,586.51 12/14/09 63.02 61.29 5,586.71 03111/10 62.82 61.09 5,586.72 05/11110 62.81 61.08 5,586.53 09/29/10 63.00 61.27 5,586.80 12/21110 62.73 61.00 5,586.74 02/28/11 62.79 61.06 5,586.84 06/21/11 62.69 60.96 5,586.73 09/20/11 62.80 61.07 5,586.98 12/21/11 62.55 60.82 5,587.07 03/27112 62.46 60.73 5,587.10 06/28112 62.43 60.70 5,587.07 09/27/12 62.46 60.73 5,587.33 12/28/12 62.20 60.47 5,587.43 03/28/13 62.10 60.37 5,587.43 06/27113 62.10 60.37 5,587.72 09/27/13 61.81 60.08 5,587.22 12/20/13 62.31 60.58 5,587.91 03/27114 61.62 59.89 5,587.74 06/25114 61.79 60.06 5,587.76 09/25114 61.77 60.04 5,587.88 12/17114 61.65 59.92 Water Levels and Data over Time White Mesa Mill -Well TWN -16 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,651.07 5,652.70 1.63 100 5,603.34 11104/09 49.36 47.73 5,603.56 12/14/09 49.14 47.51 5,603.84 03/11/10 48.86 47.23 5,604.31 05111110 48.39 46.76 5,604.28 09/29/10 48.42 46.79 5,604.39 12/21/10 48.31 46.68 5,604.20 02/28111 48.50 46.87 5,604.55 06/21111 48.15 46.52 5,604.74 09/20/11 47.96 46.33 5,604.94 12/21/11 47.76 46.13 5,604.84 03/27112 47.86 46.23 5,604.85 06/28/12 47.85 46.22 5,604.99 09/27/12 47.71 46.08 5,605.10 12/28/12 47.60 45.97 5,605.22 03/28/13 47.48 45.85 5,605.11 06/27113 47.59 45.96 5,605.39 09/27113 47.31 45.68 5,604.99 12/20113 47.71 46.08 5,605.71 03/27/14 46.99 45.36 5,605.16 06/25/14 47.54 45.91 5,605.10 09/25/14 47.60 45.97 5,605.25 12117114 47.45 45.82 Water Levels and Data over Time White Mesa Mill-Well TWN -18 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,643.95 5.645.45 1.50 100 5,586, 5 11/02/09 58.60 57.10 5,600.14 12/14/09 45.31 43.81 5,587.36 03/11/10 58.09 56.59 5,587.71 05/11110 57.74 56.24 5,587.50 09/29/10 57.95 56.45 5,607.66 12/21110 37.79 36.29 5,587.35 02/28/11 58.10 56.60 5,587.71 06/2111 1 57.74 56.24 5,587.65 09/20/11 57.80 56.30 5,587.95 12/2111 1 57.50 56.00 5,587.05 03/27/12 58.40 56.90 5,587.05 06/28112 58.40 56.90 5,587.50 09/27/12 57.95 56.45 5,587.50 12/28112 57.95 56.45 5,587.32 03/28/13 58.13 56.63 5,586.95 06/27/13 58.50 57.00 5,587.02 09/27/13 58.43 56.93 5,586.26 12/20113 59.19 57.69 5,586.87 03/27/14 58.58 57.08 5,586.23 06/25/14 59.22 57.72 5,586.02 09/25/14 59.43 57.93 5,585.99 12/17/14 59.46 57.96 Water Levels and Data over Time White Mesa Mill-Well TWN-19 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,659.59 5,661.36 1.77 110 5,606.17 11/02/09 55.19 53.42 5,606.70 12114/09 54.66 52.89 5,607.22 03111/10 54.14 52.37 5,607.89 05111/10 53.47 51.70 5,607.98 09/29/10 53.38 51.61 5,608.41 12/21/10 52.95 51.18 5,608.49 02/28111 52.87 51.10 5,608.60 06/2111 1 52.76 50.99 5,609.17 09/20/11 52.19 50.42 5,608.90 12/21/11 52.46 50.69 5,608.87 03/27/12 52.49 50.72 5,608.86 06/28/12 52.50 50.73 5,608.86 09/27/12 52.50 50.73 5,608.86 12/28/12 52.50 50.73 5,609.17 03/28/13 52.19 50.42 5,608.88 06/27/13 52.48 50.71 5,608.92 09/27/13 52.44 50.67 5,608.46 12/20/13 52.90 51.13 5,608.88 03/27/14 52.48 50.71 5,608.33 06/25/14 53.03 51.26 5,608.11 09/25114 53.25 51.48 5,608.36 12/17/14 53.00 51.23 Water Levels and Data over Time White Mesa Mill -Well MW -30 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,613.34 5,614.50 1.16 110 5,534.92 10/24/2006 79.58 78.42 5,535.09 3/16/2007 79.41 78.25 5,535.46 8/27/2007 79.04 77.88 5,535.06 10/15/2007 79.44 78.28 5,535.78 3/15/2008 78.72 77.56 5,536.26 6/15/2008 78.24 77.08 5,536.35 9/15/2008 78.15 76.99 5,536.68 11115/2008 77.82 76.66 5,535.42 3/15/2009 79.08 77.92 5,537.11 6/30/2009 77.39 76.23 5,536.93 9/10/2009 77.57 76.41 5,537.23 12/11/2009 77.27 76.11 5,537.59 3/11/2010 76.91 75.75 5,537.85 511112010 76.65 75.49 5,538.37 9/29/2010 76.13 74.97 5537.70 12/21/2010 76.8 75.64 5537.67 2/28/2011 76.83 75.67 5538.31 6/2112011 76.19 75 .03 5538.15 9/20/2011 76.35 75.19 5538.42 12/21/2011 76.08 74.92 5538.54 3/27/2012 75.96 74.8 5538.60 6/28/2012 75 .9 74.74 5538.68 9/27/2012 75.82 74.66 5538.99 12/28/2012 75.51 74.35 5539.25 3/28/2013 75.25 74.09 5539.05 6/27/2013 75.45 74.29 5539.60 9/27/2013 74.90 73.74 5539.67 12/20/2013 74.83 73.67 5539.77 3/27/2014 74.73 73.57 5539.40 6/25/2014 75.10 73.94 5539.19 9/25/2014 75.31 74.15 5539.30 12/17/2014 75.20 74.04 Water Levels and Data over Time White Mesa Mill-Well MW-31 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,615.26 5,616.40 1.14 130 5,544.07 10/24/2006 72.33 71.19 5,544.45 3/16/2007 71.95 70.81 5,536.94 8/27/2007 79.46 78.32 5,544.62 10/15/2007 71.78 70.64 5,545.37 3/15/2008 71.03 69.89 5,544.50 6/15/2008 71.90 70.76 5,545.94 9/15/2008 70.46 69.32 5,546.42 11/15/2008 69.98 68.84 5,546.03 3115/2009 70.37 69.23 5,546.65 6/30/2009 69.75 68.61 5,546.45 9110/2009 69.95 68.81 5,546.75 12/1112009 69.65 68.51 5,547.09 3111/2010 69.31 68.17 5,547.41 5/1112010 68.99 67.85 5,547.28 9/29/2010 69.12 67.98 5547.45 12/2112010 68.95 67.81 5547.37 2/28/2011 69.03 67.89 5547.96 6/2112011 68.44 67.3 5547.65 9/20/2011 68.75 67.61 5548.34 12/2112011 68.06 66.92 5548.30 3/27/2012 68.10 66.96 5548.40 6/28/2012 68.00 66.86 5548.59 9/27/2012 67.81 66.67 5548.91 12/28/2012 67.49 66.35 5549.14 3/28/2013 67.26 66.12 5548.90 6/27/2013 67.50 66.36 5549.25 9/27/2013 67.15 66.01 5549.16 12/20/2013 67.24 66.10 5548.95 3/27/2014 67.45 66.31 5548.60 6/25/2014 67.80 66.66 5548.19 9/25/2014 68.21 67.07 5548.25 12/17/2014 68.15 67.01 TabG Laboratory Analytical Reports American West ANAIYT 1CAI lAAORATORlFS 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. 4th Quarter Nitrate 2014 1410138-010 Client Sample ID: Piez-01_10082014 Collection Date: 10/8/2014 1302h Received Date: 10/10/2014 1030h Analytical Results Date Compound Units Prepared Chloride rng/L Nitrate/Nitrite (as N) rng/L Date Analyzed 10/13/2014 1350h 10/10/2014 1724h Contact: Kathy Weinel Method Reporting Analytical Used Limit Result Qual SM4500-CI-E 5.00 57.6 E353.2 0.100 5.75 Report Date: 10/27/2014 Page 13 of20 All analyses IJN~It«;abfc-w t'J)Q '\\ .. .A. .SriWA. amlRatA ftJ'ft'il,nmd UI.Jct.·ordance UJ ~t:l.A pn'KOi!bl Pertinenl sompling infool'talll\(1 n lpr-l;uiich.w the ott.ached Cl)C ·~fltltnll.,llJ\nbwo.lurf!•'~ This report is provided for the exclusive use oflhe addressee. P1 tiler'.-ltl ~ttwtq,UU.t\l tJKvflhf t,um\t ol'lhb t~tlfl::zu 4.N Cfl.)' mernber or u~ ~tllft.l,lf NrnM\u\tion of llu& report in Ulflnrat!lf' ~t•h t.beiJJ~\"rtiscmenl, promotintt (d .. leur u~· JU(\4fllt1 fitp~ or in connection with the re-publication of this l'eport for any purp ~.ei)JIJN 1l10o '1(1' lhC't»dd~ wAll!~ ,unrmta.J nn\1 m1 C'I"W''ib(1. This com1•N1 'M'«'flltllL'flts(t(M•sibilily except for U~Uuc (N:!tf1UliUU1«1 nflnspecLion and/01 111111'~' m gf,., rnhf1Jtl'\a.l~ttllll1 ttl Lhe rules of the tmde and of science. American West ANALYTICAl I ABOAATORifS 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Nitrate 2014 Lab Sample ID: 1410138-011 Client Sample ID: Piez-02_10082014 Collection Date: 10/8/2014 1240h Received Date: 10/10/2014 1030h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 10/13/2014 1354h 10/20/2014 1510h Contact: Kathy Weinel Method Reporting Analytical Used Limit Result Qual SM4500-Cl-E 5.00 12.2 E353.2 0.0100 0.755 Report Date: 10/27/2014 Page 14 of20 All analyses f"'iilh::~lhrotA the CWA, SDWA1 ~fl.l (t(,,:tA W'C' l~(,'lll.J,l(d t ~~tocrordance to l\ELAC pr.itor& rtttiu.ctlt MlllPIIHS information is located on the attached COC. Confidential Business lnfonnaLion: This report is provided for the exclusive u6e of the addressee. Pth l~t:i M ~bsequent use of Lhc t11ti'UI (!(Tln'll t1)1np;rt~ <'lr IIU' member of its staff, Of ~hli!'t;on ~(d)h rrpm1 Itt connection with the advertisemenL, promotion or sale of ony product or process. or in connection with Lhe re-publication oftllis report forany purpo:k '-'lin ltJJn forthe addressee •IO'hc-tr&lllt4l'rftlt •"''• ~,.,.This compan>· accepb-OO«nuttu:l.hiiJ.h ~~ fttrthe due perfonmmce of inspection and/or analysis in good foiLh and according Lo lhe rules ofth~: trade ond of science American West l1f'JAl YTICAl I ADORATOAirS 3440 South 700 West Salt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. 4th Quarter Nitrate 2014 1410138-012 Client Sample ID: Piez-03_10082014 Collection Date: 10/8/2014 1250h Received Date: I 0/10/2014 I 030h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 10/13/2014 1355h 10/10/2014 1709h Contact: Kathy Weinel Method Reporting Analytical Used Limit Result Qual SM4500-C1-E 5.00 28.3 E353.2 0.0100 1.74 Report Date: 10/27/2014 Page 15 of20 All analyses applicnble lo the CWA, SDWA, and RCRA are perfonned in accordance to i\ELAC protocols Pertinent sampling infonnalion is localedon the atlached CDC Confidential Business lnfonmnion: T11is rt'pOLt is provilled for Lhe exclusive use ofthe addressee, Privileges of subsequent use oflhe name of this company or ;my member ofils staff, or reproduction oflhis report in connection Vi ith the advertisement, promotion or sale of any product or process. or in connection with the re-publication of this 1~pm1 for any purpose olhe1 than fol the addressee will be grAnted only on conl.<lcL. This comrany aceepls no responsibility excepl for the due perfonnance of inspection <Jndfm :maly~is in good faith and According to I he rules of the trade and of science INORGANIC ANALYTlCAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Nitrate 2014 Lab Sample ID: 1410138-003 Client Sample ID: TWN-01_10082014 A" A I YTI c A I I An 0 A AT 0 R I [ s Collection Date: 10/8/2014 812h 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Received Date: 10/10/2014 1030h Analytical Results Date Compound Units Prepared Chloride mg!L Nitrate/Nitrite (as N) mg!L Contact: Kathy Weinel Date Method Reporting Analyzed Used Limit 10/13/2014 1340h SM4500-CI-E 5.00 10/10/2014 1649h E353.2 0.0100 Analytical Result Qual 27.6 1.46 Report Date: 10/27/2014 Page 6 of20 All Dna lyses IIJ,,}~~\l:ll 'lfltl fW ;. lJWA.•unJtt~RA. Anl perl'mmml in accordance to l'\8LAC f111~1' f'.t' nMI sampling h:tf~mtollilu ll.located un lt~t"WI{II~ uAt("OC. Confiden~ I\' IIUqf\'0" lrt1Uf11~111f')!l-Th1' r~ 1s provided for the exclusive use of the addr~ssee. P"'"Uc:,e. u( 'oti I!Oellutn\ wfA l ... ftiUIIt: c.1l' Uu. CUfftii!JJi\' tH' any member of its staff, 01 trtueu1uc! 1 t'ij'~is report in l'\l~14;u '.'tlh the advef11•etnmn, f!ft:RT~Otion or sale ~ f?llhQJ....t rrr • 01. ~tion with tl1e re-publication of this report for any purpOM'"'bn 1ft:ln (b~ lhct ·~~ '-'l.il' boo·6P'l\l\14._'if<•ll) lift {lilt tact This company accepc;..-1f9 to.pt,tlblhithr e:'(cepl for dox-..tur-J!'leff nee of in6F''fr•ltl nnlllur analysis in g(lrf,., fMfdlllltlhtc<O(dii'OJ ttnf~nt~• qrthe lrade and of science. American West ANALYTICAL LABOR/,TORif!> 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Nitrate 2014 Lab Sample ID: 1410138-007 Client Sample ID: TWN-02_10082014 Collection Date: 10/8/2014 1233h Received Date: 10/10/2014 1030h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg!L Date Analyzed 10/13/2014 1345h 10/10/2014 1723h Contact: Kathy Weinel Method Reporting Analytical Used Limit Result Qual SM4500-Cl-E 5.00 81.0 E353.2 1.00 70.6 Report Date: 10/27/2014 Page 10 of20 All analyses applicable to the CWA, SDWA, and RCRA Hre pNfl'1ml./'d;'" •ccordance lo t\ELAC pTOU.Il~ l1tHlfle1HH.ll,IIJlltt# l.n!onnation is located un the all<lched COC. ConfidenliRl Bllsiness Infonnation: TI1is report is pro"ided for U1e exclusive use of the addressee. Pri,•ileges of subsequent use of Lhe name of this cmnpt.tuy t11 ~ll)' member of its staff, or reph)du"'ltl11 ,,j tillt• l"Cfh'JJR n1 f.'(lOnection with the advertisement. promotioll or sale of any prlldt•ct or process. or in conneclion "ilh the re~puhlication oftl1is report for any purpose olher Lhao for the addressee will he granted only""' omtfl(1_ This company accepts no rDJ1«ftl1Mlitt t~ tbJ l~e due perfonnance of inspection nndloL analysis in good failb And according La Lhe rules of the Lmde and of science American West ANAl YTJC AI l AI10 AATORI[S 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Nitrate 2014 Lab Sample ID: 1410138-006 Client Sample ID: TWN-03_10092014 Collection Date: 10/9/2014 705h Received Date: 10110/2014 1030h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 10/13/2014 1359h I 0/10/2014 1653h Contact: Kathy Weinel Method Reporting Analytical Used Limit Result Qual SM4500-Cl-E 50.0 153 E353.2 1.00 19.1 Report Date: 10/27/2014 Page 9 of 20 All analys~s applicahle to 1he CWA. SDWA, and RCRA are perfonned in accordance to I'!ELAC protocols Pertinent sampling infonnalion is located on the altached COC Confidenlial Business lnfonna1ion: ll1is r.:port is provided for I he exclusive use of the addressee Privileges of subsequent use oflhe name of this comrany or any member oiils slaff, or reproduction of !his report in connection with I he advertisement, promotion or sale of any p1oduc1 or process. or in connection with the re-publication of this report for any purpose otlte1 than for the adlliessee will be granted only on conlacl This company accepts oo responsibility except for the due perfonnltnce of inspection 1\nd/01 nnaly~i'> in good faith and according to the rules of the trnde ond of science American West ANALYTICAL I ArlOAATCRifS 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Kathy Weinel Project: 4th Quarter Nitrate 2014 Lab Sample ID: 1410138-005 Client Sample ID: TWN-04_10082014 Collection Date: 10/8/2014 923h Received Date: 10/10/2014 1030h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Chloride mg/L 10/13/20 I 4 1342h SM4500-Cl-E 5.00 30.7 Nitrate/Nitrite (as N) mg!L 10/10/2014 1652h E353 .2 0.0100 1.44 Report Date: 10/27/2014 Page 8 of20 All analyses fl!llf11k~btt (J ibc{.W SllWA, om.t MtJIA lfC" rnn\ttmli u. .tccordance to J\'ELAC protocols. Pertinenl k.tllnr~hrtii infonlllll~ "lOcated (ln the al1.tlcfK"dt"OC ,~,....r~lqtial Business ]nfnnnatiOJl: This report lS provided for the exclusive use of the addressee. Pri\Jkff' u ~l~all.bf (lf'U.. t~mJo (lfltllk~ cU' •(\) member of its sl<lff. or reproduction of Lh1~1t'fll'n lll conn mn whit the ndverlisemenl, f11Hf1N)I(nn. tW lhk of nny product or process. or in connectio11 with the re-publica! ion oftbis report for any purp1~ Olhm dmn ~rt ,1nr t~kftc::Moe't.Yt,1l IMI ~lllfih;r.lanl tm con1~Ct. This compaoy accepts no responsibility e\«ppl~..'lil th~ dua JIC!rftl1tnllnce of inspec1ion ~Vv• ~twh111• 1n eood failh and accordi11g Lo the rules of I he lrnde and of science ANALYTICAl lABORATOP.IfS 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Kathy Weinel Project: 4th Quarter Nitrate 2014 Lab Sample ID: 1410138-001 Client Sample ID: TWN-07_10092014 Collection Date: 10/9/2014 655h Received Date: 10/10/2014 1030h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Chloride mg!L \0/13/2014 \332h SM4500-Cl-E 5.00 5.93 Nitrate/Nitrite (as N) mg/L \0/10/2014 1644h E353.2 0.0100 0.968 '-Matrix spike recoveiJ' indicates matrix interference. The method is in control as indicated by the LCS. Report Date: I 0/2 7/2014 Page 4 of 20 All analyses.ltpplh .... Jil)'tc-U.! lhc,! ~YA • .SPYoi", an,11tc.R.A....-rulh11rn;t1 in aceordnnce to l\ELAC IFinlbl\ll Pminenl sampling inflltlnlllii'MI "lncated on ll~o~;2l tliCd ' 'I\ ("f!'fiJklqml\1 pmlo,cu tnf"'JJ5011f.ullr This r~port is provided for the «.di.U·n"'=~ oflhe addressee. Pm·~•""r~~~~ u~vC.thetUUU.I tlf~h r;ooq'111•~' at Any me~ber ofiLs staff, 01 f'JMnttucunn ?~Lhis report in.....,_mn'llOll~.ilh the od~erth:tt~a'l~ ~NHihUI •rwl'l' frf JIPI)'!pwdw.-1 WJH~~ or in connection wilh the re-pl_lbln:ri(Ot!Of\his report for any rufPU..c Nhc:t lh•m f!IC il1c: p,fl,JC\ * wUI 'IC' 8"'\llflf oofy1m m,tact. Th•s ~ompany acceph yw; 1 \Ullhly excepl for t~dbe rerfbtlrunce of mtprttu1ft ilfJ(Wf llnlii)'U.! ~llt'~l f•nh Md"I«1Jfl m,: ''' Lhe rules of the trade ond of sct_.t~ INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Nitrate 2014 Lab Sample ID: 1410138-002 Client Sample ID: TWN-07R-10082014 ANAtvr•cAL tAoe>R•roRtrs Collection Date: 10/8/2014 729h 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Received Date: 10110/2014 1030h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Contact: Kathy Weinel Date Method Reporting Analytical Analyzed Used Limit Result Qual 10/23/2014 1444h E300.0 1.00 < 1.00 10110/2014 1648h E353.2 0.100 < 0.100 Report Date: 10/27/2014 Page 5 of20 All aualyses <~pplicable to the CWA, SOW A, and RCRA are perfonned in accordance to l\CLAC protocols. Pertinent sampling infonnation is located on the auached COC Confidential Bu:;;in.:ss lofonnation; TI1is r~pDit is provided for the exclusive use of the addressee Privileges of subsequent use of the o<1me of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process. or in connection with the re-publication of this repor1 for nny purpru;e olher than fOL the addressee will be gmnted only on contacl. This company accepls no respomibility excepl for Lhe due perfonnance of inspection nnd/o• analysis in good faith and according to the rules of the trnde and of science 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Nitrate 2014 Lab Sample ID: 1410138-004 Client Sample ID: TWN-18_10082014 Collection Date: 1 0/8/2014 84 7h Received Date: 10/10/2014 1030h Analytical Results Date Compound Units Prepared Chloride rng/L Nitrate/Nitrite (as N) rng/L Date Analyzed 10113/2014 1341h 10/10/2014 1651h Contact: Kathy Weinel Method Reporting Analytical Used Limit Result Qual SM4500-Cl-E 5.00 74.8 E353.2 0.0100 1.47 Report Date: 10/27/2014 Page? of20 All analyses ~~~II: , .. to tl'C c \ :1\.aSlJW • "nd Rt:AA .-.a pcdrmnt\l rn JICCOrd.<\nce to l'\ELAC protocols. Pertinent sampling lilr(Km)llob '-klc:lttd on the 11\AC!bc~ C.'PL' ConfidentiAl Bw;;in~"lli(l;lfR'IIII~n: T1ti• r"J"''A" k provided for lhe e:~clusive use of the addressee. PrpW"IIIi'frl.-f s1 tc.-,uem tj,M' ~,ra.hf ''"'~ N"ahh-~(!f"rtpm ur anY member of iLs s~ff, or reproduction of this r.:port iu 4.\ilU'W't'hr)n l.th Hv.: adverti~lt'IMil.jYUUt\ll.fon or sale of any prodiluu• P'ie<ss. nr hi onn:ction with the re-puhlication of this report for any purpu 1\lhtr lllan lor 1f..,L1~ Y.-111 bcutfl'lttlr.rt Oll1) 011 t;;uuw~-t. This compony accepts no respousibilily ~xcepl for IJw'tJue l•tftm11.J.l)Cbof inspec.ibtt m~llfi.\r onaty.sis in good foilh nnrt"IJ;.;~dult; to the m1"" "(the Lrade and of science. 3440 South 700 West Salt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-Jabs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Chloroform 2014 Lab Sample ID: 1410353-003 Client Sample ID: TW4-22_1 0212014 Collection Date: 10/21/2014 1313h Received Date: 10/24/2014 950h Analytical Results Date Compound Units Prepared Chloride mg!L Nitrate/Nitrite (as N) mg/L Date Analyzed 1112/2014 1320h 11 /3/2014 1119h Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual E300,0 100 596 E353.2 10.0 54.9 Report Date: 11/12/2014 Page 9 of 55 usn~, ~ to~ ~\.~ow ~ ft ~~~~"' K:(~ W!\ {" ~~ rcr.ttl)t(:(il sampling infOJm~D is located on lhe allachcd COC. Confidential Bu!ilocss lnfonmJLion: This report is prm·idcd fOf'"thc cxclusi\"C usc oflhe IIJdr~ ,,fit ltqo ·~ ·~ tbC of .. n.arne or UJit ftMHp=n .., ~ :rolh.T or~.~., cu{f « ~KNI of l.his report io COflllCC(fOO \\ ilh the ach·crtiscmeot, promotion Of sale of an} producl or process. or in coonoct.im \lith I he re-publication of lhis report ldt"Mt\ ~ :"'o.fto'..n \b• R-t W~"iflk(l"•lfQI:i(ll~ ffJIIC('pflfk:l Th\1\C'I'.iftf~ l«q~(IO~~ \ cxcepl forlheducpcrfonnaoccofiosp..--ct~nand/orOJoalysisl.n,good. failh and according lolhcrulcsoflhc trade and of science. INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Chloroform 2014 Lab Sample ID: 1410353-002 Client Sample ID: TW4-24_10212014 ANALYT'CAL • AeoRATORifs Collection Date: 10/21/2014 1305h 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Received Date: 10/24/20 14 950h Analytical Results Date Compound Units Prepared Chloride mg!L Nitrate/Nitrite (as N) mg!L Contact: Garrin Palmer Date Method Reporting Analytical Analyzed Used Limit Result Qual 11/2/20 14 1303h E300.0 100 1,050 11/3/2014 1118h E353 2 10.0 35.7 Report Date: 11/12/2014 Page 8 of 55 All .l:blh~~lk:l!r.cle:UIIC :\.'.\ )\\'A Atilt M AA oiK '"'""'(1-Jrmod 1n •c«..sara:;\ \If {'' ~ r u ~pl&:t;.a.ul'\3JnuJ.kw ... \uot.cdiWt dl.:~l.llhfd coe t...onlldr Ill Fkmr.::u lntbrrnalion: This report isprovKtcd for lhec:\Tiusi\·e uscoflhc ~ Vm·~~"'o.r~...,.W"<O(II ~(,(IJI:i uttapW-. lY.ttl'l muubr.:t.o!~ Jrt<ll ~·:uonQ(It f\1 1in HC1I'XfOQ{ln~Mhll~e~~ &iCQC1 ~0J&;aki.JfSfl) sn · torproccss.orinconncclionwilhthcn:--pubiK-ationoflhls report f1H.,. ~WI"""OII>a duoll>r 1/t-~ ~ III l-o Jll'lll'«l \• ""«"!!X< 0.• ...,,po.,) aa<pa"" "'''>ll"bolon ,~ (dr d1<' p:l(,_ orm• l!v" ...d. r ..W•1i>m~ ll!llh end acC<J<ding to the rules or lhe lt3dc and or science 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 4th Quarter Chlorofonn 2014 Lab Sample ID: 1410353-001 Client Sample ID: TW4-25_10212014 Collection Date: 10/2112014 1252h Received Date: 10/24/2014 950h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Chloride mg/L I 1/5/2014 2310h E300.0 10.0 58.1 Nitrate/Nitrite (as N) mg/L I 1/3/2014 1037h E353.2 0.100 1.03 1-Matrix spike recovery indicates matrix inteiference. The method is in control as indicated by the LCS. ReponDate: 11 /1212014 Page 7 of5S d ~"'•"'IP.'ko!JI<:Wthc ~·.-. Sb\1' ,ond M llAV<pm•li!Mlm""-w, t;I.,\Cpoi<I<Vi.,l'mn><ntsampling infmnalioo is located on the anacJIC4(.0C'" l" li:i<:folooll.li :i\klfDf....-Tlil>t<p<>n r~provld<il ((I< tll<«<fUtll'<'""vftbt Ill"""""' Pnukt>-.., of «•~ u>c tbt...., Ql <lid tClJI'P'"' t.tr.l!>) onrnt!xtof IU 1urr. ·~ "iJ1f«baiP"•>f lflis report in cOilll<lCtion with the advertiscmenL jioUIJI<l(j<.,oW «ko( ~~~ ~t<r.l..ct 01 IN\""'». <X"' ltlmJ;:ctu>n •llh tl~e •<1'0hlk.,.. tthit tl r1 ru-P<'l vt!Jathm nx d.,~ c .. l!ll><p.; ;;d<Wlb """"....,. Ths~ .cat•< non <IIUt except ror~teduep;:normanceofinsl""<tion DQII/oi<IIAI"'"''"' If., ~ ....,.lim "'llll!•uboftho•r><I<.OOof""""" American West ANALYTIColl IABORATORJfS 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 e-mail: awal@awal-Iabs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Chloroform 2014 Lab Sample ID: 1410353-020 Client Sample ID: TW4-60_10232014 Collection Date: 1 0/23/2014 830h Received Date: I 0/24/2014 950h Analytical Results Date Compound Units Prepared Chloride mg!L Nitrate/Nitrite (as N) mg!L Contact: Garrin Palmer Date Method Reporting Analyzed Used Limit 11/2/2014 2146h E300.0 1.00 11/3/2014 1117h E353 2 0.100 Analytical Result Qual < 1.00 <0.100 Report Date: 11/12/2014 Page 26 of 55 All aruJI)SCS applicable to the CWA. SDWA. and RCRA an: J"."'ffonncd in accordance to NELAC protocas Pcrtinml sampling informabon is loca.aed m lhe au.ached COC Confldcntia.J Business lnfoon::~lioo: This report is prO\ idcd for the cx.clusi\·e use of the add.rcs9:c Pri'ilegcs of subscqocnt use of the name of this company or~· Rh.."Trl.th::r of ilS staff. or rcprcxb=tton of this report in comcctioo u il.b I be advcrtisemc:rrt., p-omotion or sale of illl}" producL or process. or in rooncxlion "ilh lhc re-publiclltion of this rep:m for all) purpose other lh311 for lhc addressee "iJI be granted only on conlad Th.isrornpar~ accepts no n.~bilil) e:w~ focllrduc pcrfomtaDCc ofinspxtioo and/or aalysis in good faith and according \o lhc rulcsoflhc trade and ofsc~ American West ANAlYTICAl I A[iORATORifS 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 l) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Nitrate 2014 Lab Sample ID: 1410138-009 Client Sample ID: TWN-60_10082014 Collection Date: 10/8/2014 645h Received Date: 10110/2014 1030h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg!L Date Analyzed 10/23/2014 1534h 10/10/2014 1702h Contact: Kathy Weinel Method Reporting Analytical Used Limit Result Qual E300.0 1.00 < 1.00 E353.2 0.100 < 0.100 Report Date: 10/27/2014 Page 12 of20 All analyses applicable to the CWA. SDWA, and RCRA are perfonned in ac..:ord.Rnce lo KELAC pTOtocols Pertinent s.~mpling infonnation is located on the alt.ached COC Confidential Busin~ss lnfonnation: T11is report is provided for lbe exclusive use of the addressee_ Privileges l.lf subsequent use oflhe name of this company or any membe1 of its staff, OJ reproduction of this report in connection with tbe ftdvertisement.. promotion or sale of any prl.'lduct or proces~. or in connection wilh the re-publication of this report fo1 any purpose olher than f01 the adtlr~ssee will be gmnted only on conlact This comp<my ACCepts no responsibility excepl for lhe due perronnance of inspection and/01 analy.cois in good faith t~nd according to the rules of the trade ond of science 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Nitrate 2014 Lab Sample ID: 1410138-008 Client Sample ID: TWN-65_10082014 Collection Date: 10/8/2014 847h Received Date: 10110/2014 1030h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 10/13/2014 1347h 10/10/2014 1728h Contact: Kathy Weinel Method Reporting Analytical Used Limit Result Qual SM4500-CI-E 5.00 72.3 E353.2 0.0100 1.47 Report Date: 10/27/2014 Page II of 20 All analyses applicable to tht! CWA, SDWA, and RCRA ore perfonned in at:cordance La NELAC pmtocols Pertinent sampling infonnation is located on the attached COC, Confidential Business lnfonnation: This report is provided for U1e e:<clusi\'e use of the addressee Privileges of subsequent use of the name of this company or ~oy 1nember of its staff, or reproduction oftbis report ia connection \\ ith the advertisement, promotiou 01 sale of any product or process. or in conneclion with lbe re-publication of this report for any purpo~e other than f01 the addr~ssee will be gran led only on conl<'ICL, This compomy acceplii no responsibility except forth~ due perfcmnance of inspection ancVor analysis in good failh and according Lo the rules of Lht: lrnde and of science Kathy Weinel Energy Fuels Resources, Inc. 1050 17th Street, # 950 American West Denver, CO 80265 ANAlYTICAl I ABORATORtrS 3440 South 700 West Salt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer TEL: (303) 389-4134 RE: 4th Quarter Nitrate 2014 Dear Kathy Weinel: Lab SetiD: 1410138 American West Analytical Laboratories received 12 sample( s) on 10110/2014 for the analyses presented in the following report. American West Analytical Laboratories (AWAL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging fficiency. TI1e 11Reporting Limit" found on the report is equivalent to the practical qu.amitati n limit (PQL). This is the minimum concentration that can be rcp01ted by lhe method referenced and the . ample matrix. The reporting limit must not be confu ed wHh any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Approved by: Digitally signed by Jose G. J 0 S e G ~~~hc~=Jose G, Rocha, • o=American West Analytical Laboratories, ou, R 0 c h a ~~~~=jose@awal-labs.com. Date: 2014,10.27 12:46:35 -06'00' Laboratory Director or designee Report Date: 10/27/2014 Pagel of20 All IIUJI\)'~ 1t['l'lllrll'l'lrC1 lb 1h: WA.. SD\\~A, .w.U R AA rue fWrll'ln'lk'a. If~ ot'QI'f~btKc t~ 1'\ELAC protocols. ~ertinen! utrmlm~ ~l'lfilnllllt'-OJI n~~Witd on ~e ',llt;,tHlt\I.COt Confidentiol Business lnfonnation: Th'£6 h:fM n prov~ded for the ex_clu~ive use ?f the addtf' ~· h ~%!~(• tlhilh~umt 1 o( lhc mrm:" 1)(\tuacOulJim> or •'?-mm~JCi vf 1ts staff, or reproductton ofthuj ~ t~ "~~,u1u W,lh Ulr adverllst'llK"111, IKumotton or sale of any product or process. • '" C'6JJII«lion w1th 1he re-publtcHlton of l111s report for 1111.}' VH~()Jhcr dliln (llfl'he~l.ttu« wLtll.t ~me<Jwrl)ttm CU~Mts•tL 1 ht.. i:001pany accepL<; no responsibility~~ fM ' ,tut PTG llAtiCt-of inspe(1JC&Il t.Udllll :~nalysis in good failh and according to ilic llllo •)ftlte trnde and of sciellce. SAMPLE SUMMARY Client: Energy Fuels Resources, Inc. Contact: Kathy Weinel ANAlYTICAl LABORATOAIFS Project: 4th Quarter Nitrate 2014 Lab Set ID: 1410138 Date Received: 10/10/2014 1030h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 3440 South 700 West 1410138-001A TWN-07_10092014 10/9/2014 655h Aqueous Chloride, Aqueous Salt Lake City, UT 84119 1410138-00lB TWN-07_10092014 10/9/2014 655h Aqueous Nitrite/Nitrate (as N), E353.2 1410 13 8-002A TWN-07R-10082014 10/8/2014 729h Aqueous Anions, E300.0 1410138-0028 TWN-07R-10082014 10/8/2014 729h Aqueous Nitrite/Nitrate (as N), E353.2 Phone: (801) 263-8686 1410138-003A TWN-01_10082014 10/8/2014 812h Aqueous Chloride, Aqueous Toll Free: (888) 263-8686 1410138-0038 TWN-01_10082014 10/8/2014 812h Aqueous Nitrite/Nitrate (as N), E353.2 Fax: (80 1) 263-8687 1410138-004A TWN-18 10082014 10/8/2014 847h Aqueous Chloride, Aqueous 1410138-0048 TWN-18 10082014 10/8/2014 847h Aqueous Nitrite/Nitrate (as N), E353.2 e-mail: awal@awal-labs.com 1410138-005A TWN-04_10082014 10/8/2014 923h Aqueous Chloride, Aqueous 1410138-0058 TWN-04_10082014 10/8/2014 923h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 1410138-006A TWN-03_10092014 10/9/2014 705h Aqueous Chloride, Aqueous 1410138-0068 TWN-03_10092014 10/9/2014 705h Aqueous Nitrite/Nitrate (as N), E353.2 1410138-007 A TWN-02_10082014 10/8/2014 1233h Aqueous Chloride, Aqueous Kyle F. Gross 1410138-0078 TWN-02_10082014 10/8/2014 1233h Aqueous Nitrite/Nitrate (as N), E353.2 Laboratory Director 1410138-008A TWN-65_10082014 10/8/2014 847h Aqueous Chloride, Aqueous 1410138-0088 TWN-65 10082014 10/8/2014 847h Aqueous Nitrite/Nitrate (as N), E353.2 Jose Rocha 141 0138-009A TWN-60_10082014 10/8/2014 645h Aqueous Anions, E300.0 QA Officer 1410138-0098 TWN-60 _1 0082014 10/8/2014 645h Aqueous Nitrite/Nitrate (as N), E353.2 1410138-0IOA Piez-0 I o---1 0082014 10/8/2014 1302h Aqueous Chloride, Aqueous 1410138-0108 Piez-01 10082014 10/8/2014 1302h Aqueous Nitrite/Nitrate (as N), E353.2 1410138-011A Piez-02 _1 0082014 10/8/2014 1240h Aqueous Chloride, Aqueous 1410138-011B Piez-02_10082014 10/8/2014 1240h Aqueous Nitrite/Nitrate (as N), E353.2 1410138-012A Piez-03_10082014 10/8/2014 1250h Aqueous Chloride, Aqueous 1410138-0128 Piez-03 10082014 10/8/2014 1250h Aqueous Nitrite/Nitrate (as N), E353.2 Report Date: 10/27/2014 Page 2 of20 All analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to t\ELAC prmoco/s Pertinent sampling infonnalion is located on !he attached COC Confidentinl Business (nfunnation: This report is provided for the exclusive use of the addrt!ssee Privileges of subsequent use of the name of this company or l'IOy member ofils staff, or reproduction of this report in conoecLion with the advertisement, pro1notioll 01 Sllle of any r•oducl or process.. or in conneclion with the re-publication of this report for any purpose other than for the addressee will be granted only on contact. This compan)' accepts no responsibility except for the due perfonmmce of inspection ancVoJ analysis in good faith and according to the rules oft he lmde and of sci~uce 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Kathy Weinel Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: 4th Quarter Nitrate 2014 1410138 10110114 1018114-1019114 Intact None Holding Time and Preservation Requirements: The analysis and preparation for the samples were performed within the method holding times. The samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, LCSD, MS, MSD, RPD, DUP: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample I Laboratory Control Sample Duplicate (LCSILCSD): All LCS and LCSD recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicates (MSIMSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exceptions: Sample ID Analyte QC Explanation 1410137-003C Chloride MS/MSD Sample matrix interference 1410138-001A Chloride MS/MSD Sample matrix interference Duplicate (DUP): The parameters that required a duplicate analysis had RPDs within the control limits. Corrective Action: None required. Report Date: 10/27/2014 Page 3 of20 All analyses applicable to the CWA, SDWA, and RCRA are perf on ned in ac,;ordance,lo M.!l f prOloco._._ fl(nmllll! """l"UnJinfonn<~lion is located on the attached COC. Confidentinl Busint'ss Information: Titis r~port is provided for the exclusive use of the addressee. Privileges of subsequetU use of the name ofthi:; company or any memhet or~J.t...,.a.aJ.r. t~ ff'J)rodUJ:llutt t.~rtltl, tq.tOrtln connection with the adverlisement. promotion or .sale of any prodoct or process. or in connection with the re~publication of Lhil' 1 epo11 for any purposo! other than for the addressee will be b'Timted ooly on conlacl. Tbis compuu~ ~ffltl 00 res(t0:\"1bi1hy\\Xtqll (m lhe due performance of inspection nncVor analysis in good faith Md according to lhe rules of the trade and of science American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1410138 Project: 4th Quarter Nitrate 2014 Analyte Result Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Method MDL Reporting Limit Contact: Dept: QC Type: Amount Spiked Kathy Weinel we LCS Spike Ref. Amount %REC Lab Sample ID: LCS-R72257 Date Analyzed: 10/23/20141311h Test Code: 300.0-W Chloride 5.20 mg/L EJOO.O 0.00751 0.100 5.000 0 104 Lab Sample ID: LCS-R71952 Date Analyzed: 10/13/2014 1325h Test Code: CL-W-4500CLE Chloride 26.0 mg!L SM4500..CI-E 0.156 5.00 25.00 0 104 Lab Sample ID: LCS-R71824 Date Analyzed: 10/10/2014 1642h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.04 mg/L E353.2 0.00613 0.0100 1.000 0 104 Lab Sample ID: LCS-R72130 Date Analyzed: 10/20/2014 1458h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (115 N) 0.957 mg/L E353.2 0.00613 0.0100 1.000 0 95.7 Limits 90-110 90-110 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRer. RPD Amt % RPD Limit Qual Report Date: 10/27/2014 Page 16 of20 All u.n:tl)"!t4..-.., ti.VJ'Hbnblc ttt llhl C\VA .. SDWA, and RCRI\ mn: pt:"rf~\C11U:d Hl lliXOrd.an~ 10 ~El..I\C T'"'QH;...nl~ Ptt1lf'lltnl h:IDtpting infom1ation is located on the anached COC. Confidential Business Jnfom1ation: This report is provided for the t!xclusive use oft he addressee. Privileges of subsequent use of the na~ aft11u' c:omp:my(lf p.ny m.:rn~r of irs staff, nr rqlh'dilrllm) e~l lhi"' tt.!fl'On !h altmC'Ctinll WHh ~~.!C .uJ'I.I.,Ilito4J'nttnt.L ptO,nntion or sale of any product or process. or in connection with the re-publication of this report for any purpose other thun for the addressee will be gtanted only on contact. This COilJP.11lY p<;cq>J:< <1(1 rc'!"lnli!billry <"C<ept for the .w, f>l...i", .. m;lnC~ nr tll<P«!Ion arull~~ abftly.l< In ¢M<l fit hit ~ncl llt:A:Unlotll: to the rules of the trade and or science. American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1410138 Project: 4th Quarter Nitrate 2014 Analyte Result Lab Sample ID: LCSD-R71952 Date Analyzed: Test Code: CL-W-4500CLE Chloride 26.2 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 I) 263-8686, Toll Free: (888) 263 -8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Kathy Weinel we LCSD Spike Ref. Amount %REC 10/13/2014 1346h mg!L SM4500-CI-E 0.156 5.00 25.00 0 105 Limits 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPD Limit 26 0.804 10 Qual Report Date: 10/27/2014 Page 17 of20 Al11111nl.)"ioe. npplfC'~'blo 10 11'tt-CWA, SDWA. :rmd R.CRt\ 'IIC I'H)r-fonnr;.V ln a~~'"'C' In i\ll!t.AC"rtcHo:'llllb PL:41lnr:n' S.'UnJding inforn1ation is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use:: or the addressee. Privileges of subsequent usc of the name Q(lhiJt"~!"nJ~n.y c-r-onY member or h" ~rr.llrrc:pT"f1'bt<-tim (lllhl\ 11.-p.1r'l in «uU'l\'C11Vn wuh \he t.Uh(t'Ubcmem, ~n10tion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will~ granted only on contact. This COffij!DliY ~~~ to~• ""lkHt>lbillly «<«I~ Orr I he du~ rctl\•lmlilli!C •lr lll<rc·tnon wuiJO<" ;tlll!)y.<i, in jl<!ll<l r.,llll ftlld III:<IJnliu~ to lhe rules of the trade and of science. American West ANALYTICAl LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1410138 Project: 4th Quarter Nitrate 2014 Analyte Result Lab Sample ID: MB-R72257 Date Analyzed: Test Code: 300.0-W Chloride <0.100 Lab Sample ID: MB-R71952 Date Analyzed: Test Code: CL-W-4500CLE Chloride < 5.00 Lab Sample ID: MB-R71824 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) <0.0100 Lab Sample ID: MB-R72130 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) < 0.0100 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 10/23/2014 1254h mg!L E300.0 0.00751 0.100 -10/13/20141324h mg/L SM4500-Cl-E 0.156 5.00 -10/10/2014 1710h mg/L E353.2 0.00613 0.0100 -10/20/2014 1559h mg/L E353.2 0.00613 0.0100 Kathy Weinel we MBLK Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPD Limit Qual Report Date: 10/27/2014 Page 18 of20 All analyses applicable to the CWA. SDWA, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling infomu\tion is located on the attached COC. Confidential Business Information: This report is provided for the exclusive llSe oft he addressee. Privileges of subsequent use of the name of this company or any membet of its staff, or rep!'oduction of this repott in connection wilh the advertisement, promotion or sale of any product or proces~. or in connection with the re-publication of this report for any purpose other than t'ot the addJesset: will be gxanted only on contact This company accepts no responsibility except for the due perfom1ance of inspection and/01 analysis in good t8ith and according to the rules Clf the hade and of science ANALYTICAL LABORATOR!ES Client: Energy Fuels Resources, Inc. Lab Set ID: 1410138 Project: 4th Quarter Nitrate 2014 Analyte Result Lab Sample ID: 1410138-00lAMS Date Analyzed: Test Code: 300.0-W Chloride 5.19 Lab Sample ID: 1410137-00JCMS Date Analyzed: Test Code: CL-W-4500CLE Chloride 66.1 Lab Sample ID: 1410138-00lAMS Date Analyzed: Test Code: CL-W-4500CLE Chloride 14.6 Lab Sample ID: 1410138-001BMS Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.88 Lab Sample ID: 1410137-00JBMS Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.61 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 I) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Kathy Weinel Dept: WC Units Method MDL 10/23/2014 1501h mg/L E300.0 0.00751 10/13/2014 1326h mg/L SM4500-Cl-E 0.156 10/13/2014 1333h mg/L SM4500-Cl-E 0.156 10/10/2014 1645h mg/L E353.2 0.00613 10/I0/20141729h mg/L E353.2 0.00613 Reporting Limit 0.100 5.00 5.00 0.0100 0.0100 QC Type: MS Amount Spiked 5.000 10.00 10.00 1.000 1.000 Spike Ref. Amount 0 57.7 5.93 0.968 0.704 %REC 104 84.1 86.3 90.8 90.4 1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Limits 90-110 90-110 90-110 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 10/27/2014 Page 19 of20 Ail on~ I,~ Hnrli<llbl~ CQ ch< CWA. SO\\'A, ""~ R.CRI\ .\1~ J>i'l"i"llmmlln ~li> NEl.l\C' prOlO<'ob .. P<!rflnent samplhljl ln(<>rl\l~llnn is localed on the attoched COC. Confidential Business Information: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of the nam~<6f'thb. w.~"~W)' (lf~ll)" IU\'m~ru(•W. •aU: MrtpfOIJ\\et{On dfUth rdpat'T lli (OMCctlblt wlth.th~ l:ld\'Z1"US<:ment, promouc.n orR1T~ Q( any product or process. or in connection with the re-publication of this report for any purpose orher than for the addressee will be gtanted only on contact. This C0!11J>~ny i&CJ0<11h nn reqcOJ>Jolbllhy aecpt for tbt dlle perlhmucn<:o ofin~>ccllull Mdlllf ~>Ill lyse~ on J;OC'CI (•rrh nl.ld according ll)lhc Jlli<l' ~(the trade and of science. 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West QC SUMMARY REPORT ANALYTICAL LA80RATORIES Client: Energy Fuels Resources, Inc. Contact: Kathy Weinel Lab Set ID: 1410138 Dept: we Project: 4th Quarter Nitrate 2014 QC Type: MSD Reporting Amount Spike Ref. RPDRef. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual Lab Sample ID: 1410238-002AMSD Date Analyzed: 10/23/2014 1518h Test Code: 300.0-W Chloride 5.37 mg/L E300.0 0.00751 0.100 5.000 0 107 90-110 5.19 3.36 20 Lab Sample ID: 1410137-00JCMSD Date Analyzed: I 0113/2014 1327h Test Code: CL-W-4500CLE Chloride 65.3 mg/L SM4500-Cl-E 0.156 5.00 10.00 57.7 76.1 90-110 66.1 1.22 10 Lab Sample ID: 1410138-001AMSD Date Analyzed: 10/13/2014 1335h Test Code: CL-W-4500CLE Chloride 14.3 mg/L SM4500-Cl-E 0.156 5.00 10.00 5.93 84.1 90-110 14.6 1.52 10 Lab Sample ID: 1410138-001BMSD Date Analyzed: 10/10/2014 1647h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.92 mg/L E353.2 0.00613 0.0100 1.000 0.968 95.0 90-110 1.88 2.21 10 Lab Sample ID: 1410137-00JBMSD Date Analyzed: 10/J0/2014 1735h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.61 mg/L E353.2 0.00613 0.0100 1.000 0.704 90.6 90-110 1.61 0.124 10 ' -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Report Date: 10/27/2014 Page 20 of20 All Ja::r.d)!'ti ~lf~bW to tJao C\VA. SO\VA. fil.1lt RCRA ate' flet·igrm~ '" ACG'mituwc to Ntfl.AC ~ml()l.''''-P.:nil'\i:l\.1 J,.uur,ing infom1ation is located on the anached COC. Conti<h:ntial Business Infom1acion: This repon is provided for the exclusive use of the addressee. Privileges of subsequent usc of lhe name Qrthkt.'<Wnpttn,;" o.r :Ill)' cncmt>cntfh$~JZIO'", or n;ppxlncHon ~f1h1,. tcpm Jn C\lf\n«tmn \Yhb 1he JJI)~ enhU"'ltt'1U~ ~mlition or sale of any product or process. or in connection with the re-publication oF this report for any purpose otherthan for the addresset: will be g1 anted only on contact. This coms•MY ~cc:tpl~ II<! ""'ll''~"b'llly .-;wop1 for lhclhll:.l'(rlj)flnn,.,.ll( l""'"""<tiM w..tlorlt&l~>l·lh l)OO.I fhilh nnd "'"""' ch11g:1o the rules of the trade and of science. American West Analytical Laboratories WORK ORDER Summary Client: Client ID: Project: Energy Fuels Resources, Inc. DENlOO 4th Quarter Nitrate 2014 REVISED: 1012212o14 Samples except #2 and #9 were changed to method 4500 forCI. MC Contact: Kathy Weinel Work Order: 1410138 Due Date: 10/21/2014 QC Level: III WO Type: Project UL Denison Page 1 of2 Comments: PA Rush. QC 3 (Summary/No chromatograms). Email Group; MUST report project specific DL's: Cl @ 1 mg/L, N02/N03 @ 0.1 mg/L. EDD-Denison & LOCUS. Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1410138-00IA TWN-07_10092014 10/9/2014 0655h 10/10/2014 1030h CL-W-4500CLE Aqueous 0 df-cl 1410138-0018 N02/N03-W-353.2 ~I df-no2/no3 I SEL Anal)'tes: N03N02N -1410138-002A TWN-07R-10082014 10/8/2014 0729h 10/10/2014 1030h 300.0-W Aqueous ~ df-cl 1 SEL Analytes: CL 1410138-0028 N02/N03-W-353.2 '-./ df-no2/no3 I SEL Analytes: N03N02N 1410138-003A TWN-01 1008_2014 10/8/2014 0812h 10/10/2014 1030h CL-W-4500CLE Aqueous ~ df-cJ 1410138-0038 N02/N03-W-353.2 ~ df-no2/no3 I SEL Analytes: N03N02N -1410138-004A TWN-18 10082014 10/8/2014 0847h 10/10/2014 1030h CL-W-4500CLE Aqueous df-cJ 1410138-0048 N02/N03-W-353.2 ~ df-no2/no3 I SEL Analytes: N03N02N 1410138-00SA TWN-04_10082014 10/8/2014 0923h 10/10/2014 1030h CL-W-4500CLE Aqueous D df-cl 1410138-0058 N02/N03-W-353.2 ~ df-no2/no3 I SEL Analytes: N03N02N ---1410138-006A TWN-03_10092014 10/9/2014 0705h 10/I0/2014 1030h CL-W -4500CLE Aqueous df-cl 1410138-0068 N02/N03-W-353.2 "'I df-no2/no3 1 SEL Ana(vtes: N03N02N --1410138-007A TWN-02_10082014 10/8/20141233h 10/10/2014 1030h CL-W -4500CLE Aqueous ' df-cl 1410138-0078 N02/N03-W-353.2 ~ df-no2/no3 1 SEL Analytes: N03N02N 1410138-00SA TWN-_65 10082014 10/8/2014 0847h 10110/2014 1030h CL-W -4500CLE Aqueous D df-cl 1410138-0088 N02/N03-W-353.2 ~ df-no2/no3 . I SEL Analytes: N03N02N 1410138-009A TWN-60_10082014 I 0/8/2014 0645h 10/10/2014 1030h 300.0-W Aqueous ~ df-cl I SEL 1lhalyt1!S: CL 1410138-0098 N02/N03-W-353.2 df-no2/no3 I SEL Analytes: N03N02N Printed: 10/22/2014 FOR LABORATORY USE ONLY [fill out on page 1]: %M 0 RT 0 CN 0 TAT 0 oco HOK ___ _ HOK ___ _ HOK ___ _ COC Emailed ______ _ WORK ORDER Summary WorkOrder: 1410138 Page 2 of2 Client: Energy Fuels Resources, Inc. Due Date: 10/21/2014 SampleiD Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1410138-010A Piez-01 10082014 10/8/2014 1302h 10/10/2014 1030h CL-W-4SOOCLE Aqueous u df-cl 1410138-0108 N02/N03-W-353.2 j,.t] df -no2/no3 I SEL Analytes: N03N02N 1410138-011A Piez-02 10082014 10/8/2014 1240h 10/10/2014 1030h CL-W-4500CLE Aqueous I_ df-cl 1410138-0118 N02/N03-W-353.2 br' df-no2/no3 I SEL Analytes: N03N02N 1410138-012A Piez-03 _1 0082014 10/8/2014 1250h 10/10/2014 1030h CL-W-4SOOCLE Aqueous cJ df-cl 1410138-0128 N02/N03-W-353.2 ~ df-no2/no3 I SEL Analytes: N03N02N Printed: 10/22/2014 FORLABORATORYUSEONLY[filloutonpage1]: %M 0 RTO CN 0 TATO QCO HOK ___ _ HOK ___ _ HOK_ _ _ _ COC Emailed ______ _ \ ' ~ American West Analytical Laboratories 463 W. 3600 S. Salt Lake City, UT 64115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 L~~ Fax# (801) 263-8687 Email awal@awal-labs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Contact: Gartin Palmer Phone#: (4351678-2221 Cell#: gpaiiliei@eiiez"Dfilels.comj KWeliiei@energyfu.etS.<:om; Email: tfturli!D)ca8>Dfu.als.com Project Name: 4th Quarter Nitrate 2014 Project#: PO#: Sampler Name: Gartin Palmer Date SampleiD: Sampled 1 TWN-07_10092014 10/9/2014 1 TWN-07R_10082014 10/8/2014 ~ TWN-01_10082014 10/8/2014 • TWli'-18_10082014 10/8/2014 > TWN-04_10082014 10/8/2014 ~ TWN-03_10092014 10/9/2014 7 TWli'-02_10082014 10/8/2014 ~ 'TWN-65_10082014 10/8/2014 g TWN-60_10082014 10/8/2014 0 Piez-01_10082014 10/8/2014 \ Piez-02_10082014 10/8/2014 ~ Piez-03_10082014 10/8/2014 ~ r"i'emp Blauk ~linquishedby: {:;;I~ p~ Stgnature ~~ o!tl"\ol q_ I p .. J' ~ Ptt-d,Name: k~:..r .. : .-Pe..l oA~ Time: L:300 !Relinquished by; Oate: Signature rnme: Pr:ln!N.ame; Relinquished by: Date: lsionature PtintNarne.:. Tlni;..--- R,elinquished by: ----Dafe: Slanetl.re ---:-:__ nme: Prlhi..Namc. ·r I Time Sampled 655 729 812 847 923 705 1233 847 645 1302 1240 1250 Recervedby: Sl~nature 1'11ht tlon"" ~or. :s.....- :;.,.,. H~mt' CHAIN OF CUSTODY All ana.~le wiU be conducted using NELAP accredited methods and all data will be reported usklg AWAJ...'s standard anatyto Usts and reporting Umlb (POL) unless specincally requested otherwise on this Chain of Custody and/or ettached documentation. QC Level: I Tum Around Time: Unless other arrangements have b9en made, signed reports will be emalled by 5:00pm on 3 Standard the day they ere due, lC Include EDD: LOCUS UPLOAD EXCEL Field Filtered For. !'or Compliance Wit!>: 0 NELAP C! RCRA 0 CWA Q SDWA [! ELAP I A2LA [J NLLAP "' 0' 0 Non-Compliance 0 ~ a 0 Other: "l ~ !:!. ... X :s .., 0 ~ ::E 0 a a Known Hazards 0 m :.: L1) ..... :!. 0 c. ('I & '5 E 0 tl .. Sample Comments .. "' :.: 2 w X X 2 w X X 2 w X X I 2 w X X 2 w X X 2 w X X ' 2 w X X I 2 w X X 2 w X X 2 w X X 2 w X X 2 w X X om•~ ----Special Instructions: ~ ------Pate: ----ime: ~ Date: e 1m a: rintName: 1 ~llf. A lo .Att J...ro n .uA ) ate: ~11°/ l L1 ~ ...... ' N Mi<£ 8-cl.J\l.N\-Tint« 'If>~ ~rJ r~n;Ji.,•: 1 L-l ll) l'3 <6 AWAL Lab Sample Set# Page 1 of 1 ru~-o~~=· ~ -1 : ~ - ~ ::~-~'U~.@f:!ft :r: '1'1._-''l..:!:"" ~ ~-~~ ~~ ... ~,~~~ slo!li>l-oow'il!¥ . ' --; :·: '' I. ,· ~. --• -. • --. . ~-.. ~4••"'l _- -~· c ':t ~ •. ,, }!!'\!~ ,3 'Th~o --·c .2.:-.{; • •! vf -=t '•i • ~ ..... . i ·'f;:,~~~'),ll: ...,= \ ~-~· ~~: }i:.i~ .~ r.. \". ~ '-I.~· .; .• ·· ll..:.,.,..;' '_.[~1::.! ·~~ "'tl" _ ... "); ..•. 11 ,, ·J I' ... ;,., .~.:.~t_.l 1 Kbanch I • ~ ~1· .I.'('?., __ ),,...,,,,....,,~ '-':,..~ ·~' L, .. s' ;(I • Wilrrln ,-.• -• r!~~··< ~ ·, "'=·-~·m~ ~·· ,, '\'---·' ' • ,11. :· _, -• :: . ·:4J4.JII'...,., . \.> .. •' ;:~~. :~· ~ ----- ' , :~ ._ ... : ~:r,.;tw..: . . _, ~(tta•a~oee,~~ ---t: ' : . . '*· . . ' l~ ~ ' ~. -,, . -~-' '··'-·'&~.!! x"' .. -• ~~·--··' .,:·-. • ·•'('' :_;-, .. N' . ·-J ~-. ·~ ·,. 1"-~-·; onsa:;:: ... -~-1 ~ ~~ -~·~--·-Pic ,~-_' ·~ .-v· _.) i;~ .. -'"'· ~ ··<-."r': . ~·~~-·~~----<· • ·~ .-~~ ,• ffl~i'i:~V ~ '~., -!=r :0-~-•• • - Itt .. --~---:"""' -,, ~~···-Coill;·O&t~~e -.. , · r ,. , -· · t~ -~· :1~1 ' ... .·;·· ~~ ~1 -~ .. "'" 1, • -• ~ .-" .. r-~ _. • .. Analysis Ammonia COD Cyanide Metals N02 &NO, O&G Phenols Sulfide TKN TPO~ Procedure: Frequency: Preservation Check Sheet s -le.SetExt, Preservative --oot l'-eOZ.. -003 -ooL\ --ex::b ,..000 pff <2 HzS04 pH<2 H2S04 pH>12 NaOH pH<2HN03 pH <2H2SO~ '-res I "0---~ 1\/P~ 1'\fe?b I -...Jflj..., I'J.e..S pH<2HCL J -, r I I If pH<2H2S04 pH>9NaOH, ZnAcetate pH <2 H~04 pH <2 HzSO~ Pour a small amount of sample in the sample lid Pour sample from Lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid -ec:n l''les I' dDR -ooeb -cdl l\JeS bleb_ I I 010 -· ~ -o 1\ Vel? t·•JR./S I I 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + .. # • The sample required additional preservative upon receipt. The sample was received unpreserved The Sample was received unpreserved and therefore preserved upon receipt. The sample pH was unadjustable to a pH < 2 due to the sample matrix The sample pH was unadjustable to a pH> __ due to the sample matrix interference Lab SetiD: \ L\ \ t)\ ~$ -0\2.- I~ I/ I I I AtHdVTICAI I ARORATCRifS 3440 South 700 West Salt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Garrin Palmer Energy Fuels Resources, Inc. 6425 S. Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: 4th Quarter Chloroform 2014 Dear Garrin Palmer: Lab Set ID: 1410353 American West Analytical Laboratories received 21 sample(s) on 10/24/2014 for the analyses presented in the following report. American West Analytical Laboratories (AWAL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. lfyou have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Rep01ting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Approved by: Ky I e F Digitally signed by Kyle F Gross • ON: cn=Kyle F Gross, o=American West Analytical Lab, ~=-tiltwfil~ Director, email=kyle@awai-G labs com, c=US ross Date:20141113 06:42:48·07'00' Laboratory Director or designee Report Date: ll/12/20 14 Page 1 of 55 llontl) "1'1 ~I ll~e('i 1'\WA,mol !tQt:,.,l.,lntm«ltriocro..boutoNEL\C protocols. Pcrtinenl"'flljll<ttg.nf~tt l~qttll'<llli<IWC.: C...llob\llol Busi..,..lnfOmlolion: This «port 15pmvid<:d fO<Ih<: cxclusi•·cuscofthc ~;« I~'' drso (Jr Wb :tfu::Ut.'Qto of,\lHt o:amc Q( 'lw: "'~'~ QC ~ Tr=m~"t.Qf il5 staff. or rq:wQ(b;bo~ ?~ lhn ~ m ttJftft((tioo ..-. ith l.he llhttlnooa: ptOOJOC;o., (II I&Ak or nn>: product or ~ess. or in coonccuoo \\ith 1hc re~blic<~tion of this rcpot1 (U. ""). PJ'Jl'>!'C•th<r th*1 fm lioo ..Jd--.~~ ba rraoi«loo!~()Jo<OWJ!l l W.cMipany accq>Osoorcsponsobihl} <'<!:<p<J<w 11>< .tlt< ~UfoonYOOO C(tll>i"~-"!''I >h 111 ood f8Jih and accordmg to lhc nolcs of the lr.Jdc ond ofscocncc. SAMPLE SUMMARY Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 4th Quarter Chloroform 2014 Lab Set ID: 1410353 Date Received: 10/24/2014 950h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 3440 South 700 West 1410353-00lA TW4-25_10212014 10/21/2014 1252h Aqueous Anions, E300.0 Salt Lake City, UT 84119 1410353-0018 TVV4-25_10212014 10/21/2014 1252h Aqueous Nitrite/Nitrate (as N), E353.2 1410353-001C TVV4-25_1 0212014 10/2112014 1252h Aqueous VOA by GC/MS Method 8260C/5030C Phone:(801)263-8686 141 0353-002A TVV4-24 10212014 10/21/2014 1305h Aqueous Anions, E300.0 1410353-0028 TVV4-24_10212014 10/21/2014 l305h Aqueous Nitrite/Nitrate (as N), E353.2 Toll Free: (888) 263-8686 1410353-002C TVV4-24_10212014 10/21/2014 l305h Aqueous VOA by GC/MS Method Fax: (801)263-8687 8260C/5030C e-mail: awal@awal-labs.com 1410353-003A TVV4-22_10212014 10/21/2014 1313h Aqueous Anions, E300.0 1410353-0038 TVV4-22_1 0212014 10/2112014 1313h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 141 0353-003C TVV4-22_10212014 10/2112014 1313h Aqueous VOA by GC/MS Method 8260C/5030C 1410353-004A TVV4-20_10212014 10/21/2014 1322h Aqueous Anions, E300.0 Kyle F. Gross 1410353-0048 TVV4-20_10212014 10/21/2014 1322h Aqueous Nitrite/Nitrate (as N), E353.2 1410353-004C TVV4-20_10212014 10/21/2014 1322h Aqueous VOA by GC/MS Method Laboratory Director 8260C/5030C 1410353-005A MVV-26_10212014 10/2112014 1328h Aqueous Anions, E300.0 Jose Rocha 1410353-0058 MVV-26_10212014 10/21/2014 1328h Aqueous Nitrite/Nitrate (as N), E353.2 QA Officer 1410353-005C MW-26_10212014 10/2112014 1328h Aqueous VOA by GC/MS Method 8260C/5030C 1410353-006A ~-04_10212014 10/21/2014 l335h Aqueous Anions, E300.0 1410353-0068 ~-04_10212014 10/21/2014 1335h Aqueous Nitrite/Nitrate (as N), E353.2 l4l0353-006C ~-04_10212014 10/2l/2014 1335h Aqueous VOA by GC/MS Method 8260C/5030C 14l0353-007A TW 4-04 _I 0212014 10/21/2014 1341h Aqueous Anions, E300.0 1410353-0078 TW4-04_102l2014 10/2l/2014 1341h Aqueous Nitrite/Nitrate (as N), E353.2 1410353-007C TW 4-04 _102120 14 10/21/2014 1341 h Aqueous VOA by GC/MS Method 8260C/5030C 141 0353-00SA TW4-19 102I2014 I0/21/2014 1415h Aqueous Anions, E300.0 1410353-00SB TW4-I9_10212014 10/21/2014 I415h Aqueous Nitrite/Nitrate (as N), E353.2 1410353-00SC TW4-19_102l2014 10/21/2014 14I5h Aqueous VOA by GC/MS Method 8260C/5030C I4I0353-009A TW4-03R_I0222014 I 0/22/20 14 1 008h Aqueous Anions, E300.0 141 0353-009B TW4-03R_10222014 10/22/20 14 1008h Aqueous Nitrite/Nitrate (as N), E353 .2 1410353-009C TW4-03R_l0222014 I 0/22/20 14 1 008h Aqueous VOA by GC/MS Method 8260C/5030C 1410353-0IOA TW4-03_10232104 I 0/23/2014 709h Aqueous Anions, E300.0 1410353-0108 TW4-03_10232104 10/23/2014 709h Aqueous Nitrite/Nitrate (as N), E353.2 Repon Dnt • 11/1·212014 l~ge 2 of55 AIL anolyses applicable to the CWA. SDWA. and RCRA an: perf<>rm<:d in acro<dancc W 'ELA(" t~OWWI>-~ h npldl5 m~--a ~ m 11>< all"""'l (()(' (~,.,,~ UUJif!C'I< lnfl>nNIKID' 1110JIC!l<ln n l"•rrul..-.!•lOt 0•< <'Xhll'•-. ..,. ... OOdrcsscc. Pril>ik-t;e:Sofsubscqucnt usc of the name ofllus company or any member ofn ;UO:ot fL"{Y~\OiillurtblJ.fCf'I'1"Ttl'c-~II(!IJ"'ilit. d:tt bd\cr11JIO'hMlllfOfnrt~CII ~Q(~} 1 uctor 1, rn 111CC1iuJ "-1lki.bc'rO··pubHc~MJMo(sb 1'C(11;Jr1 fo.-iln' purposcothcrlhan fO<Ihcadd=su:"illbc granted only oncontacL This com~ "'"J* I bdJI) ~ roll tb:<loep:i(Of!1UO(<~ft"''' onn~ ... tl)>kt•;ov.l ila»J>IWilotct•dlnJ IO Uw.'rlll:tofW.:Lr.>d<...,of Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 4th Quarter Chloroform 2014 Lab Set ID: 1410353 ANAlYTICAl tAFiO~ATORJfS Date Received: 10/24/2014 950h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 1410353-0IOC TW4-03 10232104 1 0/23/2014 709h Aqueous VOA by GC/MS Method 3440 South 700 West 8260C/5030C 1410353-0IIA TW4-12 10232014 10/23/2014 719h Aqueous Anions, E300.0 Salt Lake City, UT 84119 1410353-0118 TW4-12_10232014 10/23/2014 719h Aqueous Nitrite/Nitrate (as N), E353.2 1410353-011C TW4-12_10232014 10/23/2014 719h Aqueous VOA by GC/MS Method 8260C/5030C 1410353-012A TW4-28_10232014 I 0/23/20 14 726h Aqueous Anions, E300.0 Phone; (801)263-8686 1410353-012B TW4-28_10232014 I0/23/20I4 726h Aqueous Nitrite/Nitrate (as N), E353.2 Toll Free; (888) 263-8686 I410353-0I2C TW4-28_I0232014 I 0/23/20 I4 726h Aqueous VOA by GC/MS Method Fax; (801) 263-8687 8260C/5030C e-mail: awal@awal-labs.com 14I0353-013A TW4-32_10232014 1 0/23/20 14 73 4h Aqueous Anions, E300.0 1410353-013B TW4-32_I0232014 I 0/23/20 I4 734h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 1410353-0BC TW4-32_10232014 10/23/2014 734h Aqueous VOA by GC/MS Method 8260C/5030C 1410353-014A TW 4-13 _1 0232014 10/23/2014 740h Aqueous Anions, E300.0 1410353-0148 TW4-13_10232014 1 0/23/20 14 7 40h Aqueous Nitrite/Nitrate (as N), E353.2 Kyle F. Gross 1410353-0l4C TW4-13_10232014 I 0/23/2014 7 40h Aqueous VOA by GC/MS Method Laboratory Director 8260C/5030C 1410353-0l5A TW4-l4_10232014 I 0/23/2014 7 46h Aqueous Anions, E300.0 Jose Rocha l4I0353-0ISB TW4-l4_10232014 10/23/20 14 7 46h Aqueous Nitrite/Nitrate (as N), E353.2 QA Officer 1410353-0ISC TW4-14_I0232014 1 0/23/20 14 7 46h Aqueous VOA by GC/MS Method 8260C/5030C 1410353-0l6A TW4-36 10232014 I0/23/2014 755h Aqueous Anions, E300.0 1410353-0168 TW4-36_I0232014 I0/23/2014 755h Aqueous Nitrite/Nitrate (as N), E353.2 I4I0353-016C TW4-36_I0232014 I0/23/2014 755h Aqueous VOA by GC/MS Method 8260C/5030C 14I0353-0I7 A TW4-27 I0232014 I 0/23/20 I4 802h Aqueous Anions, E300.0 I4I0353-0I7B TW4-27_I0232014 10/23/20 14 802h Aqueous Nitrite/Nitrate (as N), E353 .2 1410353-017C TW4-27_10232014 I 0/23/20 14 802h Aqueous VOA by GC/MS Method 8260C/5030C 1410353-0ISA TW4-30_I0232014 I 0/23/2014 808h Aqueous Anions, E300.0 l410353-0l8B TW4-30 10232014 10/23/2014 808h Aqueous Nitrite/Nitrate (as N), E353.2 1410353-0ISC TW4-30_102320I4 10/23/2014 808h Aqueous VOA by GC/MS Method 8260C/5030C l410353-0l9A TW4-65 _102320 14 10/23/2014 719h Aqueous Anions, E300.0 I410353-0l9B TW4-65_10232014 I0/23/2014 719h Aqueous Nitrite/Nitrate (as N), E353.2 14I0353-019C TW4-65 10232014 I 0/23/20 14 719h Aqueous VOA by GC/MS Method 8260C/5030C 1410353-020A TW4-60_10232014 10/23/2014 830h Aqueous Anions, E300.0 1410353-020B TW4-60 10232014 10/23/2014 830h Aqueous Nitrite/Nitrate (as N), E353.2 Report .D:ue: I 1/12/20 14 j)itgt!3 0 55 AIL an.1ly""' applicoblc Lo the CWA_ SDWA_ and RCRA are performed rn accoo-dancc I<> " I ~I Pen-~U!fLolbllotJ II klca."U 011 ~I< uuc:I1N l"()(' c..ifldcn~ol """'"'» Jo(. ""'""' L flus ICllott "1'"-''i~cl (or die =I•~•• •"' afohQ addrcsscc. Pri•ileg:sorlillbscquenl usco[Lhc oamcorlhiscornpanyor~ mcmbcrofoli:lLOII".or•<l""'i<JI:IIl>llo(tiH tCttOO '"«<I<<JJ<'""' mthlb: oJ,..,,_,__ ror,;zJour ... ~ p<od;rcl nr1-'lf •n '""'"""'""'"'"""' f'll>k <>I ~"1'>" ror~·I'"'J'O"'oth..·nhan rorlhc addrcsscc "ill be gnntcdoolyoocootacL This com""'"'-""""" no ~MU, c~f..-!MM: pc.•f.....-:o<>flntpc<11on •r.l .. au(\uun f,W4fmh0nl.......,u,. ooih< nobcr Ltalolll>l<>f.ci<rl<l: 3440 South 700 West Salt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 e-mail: awa1@awa1-1abs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Client: Project: Lab Set ID: Energy Fuels Resources, Inc. 4th Quarter Chloroform 2014 1410353 Date Received: I 0/24/2014 950h Lab Sample ID Client Sample ID 1410353-020C TW4-60 10232014 1410353-021A Trip Blank Date Collected 10/23/20 14 830h 10/21/2014 Contact: Garrin Palmer Matrix Analysis Aqueous VOA by GC/MS Method 8260C/5030C Aqueous VOA by GC/MS Method 8260C/5030C Report Dat ' 1111212014 Page 4 9FSS Ill~ ... , IIPPh•::bl<·:o II>.•(WA. OW A. -1 RCll,\ .,..Tb*>llmctoolw<r"' EI.AC ptO!Il«<<~ l'".:n<O<i• -~'~tnr ·~~··-~ -..,)b.: .u.dw (()(" Conl\kloll>l l~ lor .. mnlioll IIIIo lq>Of( lOll«>' •.to: a rar<!l< .,..,, ''" ...... afl1>; -..,. l'll>~~of ~~1<ot'tbc"'""'ort1 ~oo.,.ro.""llocrofll>,..rt""l''~orlhi•~•••-..t""'".U.IkaJu:o~p<onw< tO<,.f<ot""!I'I<\IU<I_<><_..Ofm<-'""'""'''''''~~<>rdtlullt"'t r ....... plll"'"'w.. .. u .. , fo:o ~~<~ ... llt..-il!>rtl<>lml) '"'" 'llu·~ J«q'b """"f<nrnl>lhl~ ""CJII illrllta4l>:pa """""'"'""~""'''"' .. om~'"'" t.llloood ..... IL.aj; tOob<ntl oflh<ID:Ic .oil of- 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Garrin Palmer Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: 4th Quarter Chloroform 2014 1410353 10/24/2014 1 0/21-1 0/23/2014 Intact None Holding Time and Preservation Requirements: The analysis and preparation for the samples were performed within the method holding times. The samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exceptions: QC MS/MSD Corrective Action: None required. Report Date: 11112/2014 Page 5 of 55 ~n ""'-'"" •JI!)h<~c .. rk \'. SOW.\ ..s R ,ItA .... p..;fdllll<d w oc<otd:a"'""" E (".. .,. P<nl:tei!IUI!'I'lrn~ , .. r ....... .,.HS, """"''"" ~~~ .a.xbN ()1.. r ... rtdaa~Uil l1u_,...,, ... m>(kan~ This report as p<OI'idcd for the cxclusiYC usc oftbe ~...-e. rtn~()r~"'t1"&rttlt.:<tfU2: r.ll'f+a'oflfa:4:(\'lml=1) QC.-n:o ~JJb,:tofdJ;a.b11'.tttrl;'l1f~W..iif Lh'' f'f'J\'Itlll'lt\Dl(J(UIJ.D "·llb II\!' .MJ-Mi~trimlfti!Jt.ff()!:IOOCH ufc:ofAn)-pro6i~l~ IHl'CC"'i..or m connection \\llh the re-publ1rnlJon oflh1s report fclf•., J"'f!>:'O<clil>cT~"" (or~~""".Ut.:l.._.,. "*"' 'TlalsWIJll!'ll'l ~n<ll<fj-.iiJilil}~'f< ~atlll<:<iu< 1 fouqpn<,;c(an t""'W""""IIIb•n Jonlr .... >«mi.J•I)k>Uacrnlcsoftbe lrodcand of science. 3440 South 700 West Salt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801)263-8687 e-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Energy Fuels Resources, Inc. Garrin Palmer Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: Method: Analysis: 4th Quarter Chloroform 2014 1410353 1012412014 10121-1012312014 Intact None SW-846 8260CI5030C Volatile Organic Compounds General Set Comments: Multiple target analytes were observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Sun·ogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample I Laboratory Control Sample Duplicate (LCSILCSD): All LCS and LCSD recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 11112/2014 Page 6 of 55 , U ~~~ •r'e'Jnbkto lh:CW. ~W -.1 Ra-; acp.~ \n~tf;)UEL...\(' pu~~X:Utl f'ctmtclll sampling infonnalK>n is localed on the attachedCOC. Confldcnl.ial Business lnfonnaoon: This report is pro,·Mkd forthccxcJusi,·cusc oflhc ~ Pt~ ~ or ~(~~hi ll)e ar lh: n:z:UIQ ~IbiS ~t=rt:K 1m ma~T (f( lu l'lflfl. (tl 'Wf\IIJL&IIio.-. M' lhls report in COIUlCCiion \\ ith the ach·crtisemeoL, promotion or sale or Ml)" product or process. or in coonccLion \\ ith the r~-publicntion of this report rue Jl't\ llWJ'(~O'hcr~~,m (or ih4 -Jd'~ frfll k pa;&."tJ.~ a\~ ~ftUI9:W' ~ ttO r~IJiiJt\ except for Lhc due performance of inspection and/or anaJysis in good faith ;md 3CCOrding to the rules oflhc trade and of science_ ANhlYT:CAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1410353 Project: 4th Quarter Chloroform 2014 Analyte Result Lab Sample ID: LCS-R72575 Date Analyzed: Test Code: 300.0-W Chloride 5.08 Lab Sample ID: LCS-R72715 Date Analyzed: Test Code: 3000-W Chloride 5.14 Lab Sample ID: LCS-R72608 Date Analyzed: Test Code: N021N03-W-353.2 Nitrate/Nitrite (as N) 1.04 Lab Sample ID: LCS-R7290l Date Analyzed: Test Code: N021N03-W-353.2 Nitrate/Nitrite (us N) 1.06 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 I) 263-8686. Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com. web: www.awal-labs.com C SUMMARY REPORT Units Method MDL I 1/02/2014 1156h mg/L E300.0 0,00751 11/05/2014 1535h mg/L E300 0 0,00751 11/03/2014 1035h mg/L E353.2 0.00833 11/11/2014 1126h mg/L E353 2 0.00833 Reporting Limit 0.100 0.100 0.0100 0.0100 Contact: Garrin Palmer Dept: WC QCType: LCS Amount Spiked 5.000 5 000 1.000 1.000 Spike Ret: Amount 0 0 0 0 %REC 102 103 104 106 Limits 90-I 10 90-110 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDR~f. RPD Amt % RPD Limit Qual Report Date: 11/1212014 Page 48 of 55 AU nMt~.,a ,.()J\hCX'Ih1~ W U~ fWA. SOW A. and RCRA ott perfOrmed m accordll.(lC'C'" 10 f\l!"t--A(' pi1)t<X"'(lbo Pmultcm .,..ftling infomuttion IS located on the a1tached ('()('. C'onlidentlal Busmess lnform.tbUAl This report 1s provided for the e;...:clus1ve use C\fthl" addressee Pnv1leges of subs~X]ucnt use of the- mtii1CI' t~ftbr.,_ ootl~n~ (lf IU\\1 member of its stan: •rt tcgcOOuctwn of this report in c:-o•m«tlon W1llt tl~,J\c..'ftlJ.cltl¢1\t.IHC'IH\Otion or sale ofnny product or process. or in connection wtth the re-pubhcation ofH11s report for rmy purpose other than for the addrtssee will be granted only on contact This emil !IIIII\' ll<'cepiJ 110 f<ll)IQII,J bility c'cept for the ~pcrrar,nonce of inspectiona11tYII!iiN11)otA h• !j<'l'lllhlll•ltn<t li<tllrdlttil to the rules of the trade and of science ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1410353 Project: 4th Quarter Chloroform 2014 Analyte Result Lab Sample ID: MBLK-R72575 Date Analyzed: Test Code: 300.0-W Chloride <0.100 Lab Sample ID: MB-R72715 Date Analyzed: Test Code: 300.0-W Chloride <0.100 Lab Sample ID: MB-R72608 Date Analyzed: Test Code: N02!N03-W-353.2 Nitrate/Nitrite (as N) <0,0100 Lab Sample ID: MB-R7290l Date Analyzed: Test Code: N02!N03-W-353.2 Nitrate/Nitrite {as N) < 0.0100 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686. Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com. web: www.awal-labs.com C SUMMARY REPORT Contact: Garrin Palmer Dept: we QC Type: MBLK Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC I 1/02/2014 1139h mg/L E300.0 0.00751 0.100 11/05/2014 1519h mg/L E300.0 0 00751 0.100 11/03/20 14 I 034h mg/L E353.2 0.00833 0.0100 11/11/2014 1123h mg!L E353 2 0.00833 0.0100 Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPD Limit Qual Report Date: 11/12/2014 Page 49 of 55 All ~nalyses apphttlblrh? tiH:. CWA. SDWA. nnd f\(".U Ott" pctformed in nc«mJtU\OC' tr_\ NeJ-.\('" Ph1IOC01s Pertinent samphng infomtation rs located on the attached COC Contident•al Bus•ncss 1nformarion: This repon is provided for the exclus1v~ use of the addressee Pri,·ilcges of subsequent us~ of the name of this comiJ\it'\r or (ll\~ member of its start: tH' r~produtlton of this (i:poc1 m QCnlll&:t'll(lfl \Tlltllt\(-ad~~ocrt1semenl. promotion or sale of any product or process.. 01 in connection with the re~publ1cation of this rcpon for any purpose other th:ln for the addressee wlll be granted only l'IO contact Thi::;. company accepts 1W. tC$pt'l:tUnbility except for the (f\lt-pcr(ctnN~1Ce of insrc;thcn ~d'C1t ~u~lll)"'h 1~ P'<t f:llth nnd ~ccording to the rules of the trade and of science 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (80 1) 263-8686. Toll Free: (888) 263-8686. Fax: (80 1) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer ANALYTICAL LABORATORI[S ~ C SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 1410353 Dept: we Project: 4th Quarter Chloroform 2014 QCType: MS Reporting Amount Spike Ref. RPDRef. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual Lab Sample ID: 1410353-00IAMS Date Analyzed: 11/02/2014 1229h Test Code: 300.0-W Chloride 559 mg/L E300.0 0.751 10.0 500 0 58.1 100 90-110 Lob Sample ID: 141 0353-005AMS Date Analyzed: 11/02/2014 150 I h Test Code: 300.0-W Chloride 110 mg/L E300.0 0 0751 I 00 50.00 60.1 99.4 90-110 Lob Sample ID: 1410353..015AMS Date Analyzed: 11/02/20141841h Test Code: 300.0-W Chloride 88.7 mg/L E300.0 0.0751 1.00 5000 38.9 99,7 90-110 Lob Sample ID: 1410353..009AMS Date Analyzed: 11/02/2014 2113h Test Code: 300.0-W Chloride 5.15 mg/L E300.0 0.00751 0.100 5.000 0 103 90-110 -Lob Sample lD: 1410466-022AMS Date Analyzed: 11/06/2014 018h Test Code: 300.0-W -=- Chloride 5.08 mg/L E300.0 0.00751 0.100 5.000 0 102 90-110 Lob Sample ID: 1410353-00 I BMS Date Analyzed: 11/03/2014 1038h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.86 mg/L E353.2 0.00833 0.0100 1.000 1.03 82 7 90-110 Lab Sample ID: 1410353-0IIBMS Date Analyzed: 11103/20141121h Test Code: N02/N03-W-353 .2 Nitrate/Nitrite (as N) Ill mg/L E353.2 0 833 1.00 1000 161 95.3 90-110 Lab Sample lD: 1411097-00IDMS Date Analyzed: 11111/2014 I 131 h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.03 mg/L E353.2 0.00833 0.0100 1.000 0 103 90-110 1-Matrix spike recovery indicates matrix interftrence. The method is in control as indicated by the LCS. Report Date: I 1/12120 14 Page 50 of 55 All.ath·&l)''-01 apphoablr lo lhG' CWA. SDWA, and RC'RA lt'fl pctformed m llt«<n~10CC' tu 1\l:l .-\( (Ull«Ocols Pertment sampling infom1ation is located on the attached CO(' Confidential Bus mess lnfonnauon: This report is prov1dt!d for the exclus1ve usc of the addrt"SSee Pnvlleges of subsequent use of the name" of tht~fcom~t\r)3' ctt-..tn)~ member or its stnn: \'lr rvl•r-od-,..Mt.QO of this r~r11q ~~It-'" "h"lt C~ ~dvert•scmenl. promotion 01 sale of any product or process, 01 in connection with the re-publication of this report fo1 any purpose other than for the nddrcs..c;ee \.V\ll be granted only on contact Th1s cotnlllll!Y ot:«PIJ' '"' f'<'JJ><riPI!bility except for the iltt< Jlflfoom•nce of inspteuon ~t/W\'1¥ An>ly4 u\ ~~)<>J faith nnd according to the rules ot" the trade nnd of science 3440 South 700 West Salt Lake City, UT 84119 Kyle F. Gross Phone: (801) 263-8686. Toll Free: (888) 263-8686. Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com. web: www.awal-labs.com Jose Rocha QA Officer Af\oAlYTICAl l ABORr,TORIES """C SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 1410353 Dept: we Project: 4th Quarter Chloroform 2014 QCType: MSD Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual Lab Sample ID: 1410353-00IAMSD Date Analyzed: 11/02/2014 1246h Test Code: 300.0-W Chloride 562 mg/L £300.0 0.751 10.0 500.0 58 I 101 90-110 559 0.601 20 Lab Sample ID: 1410353-Q05AMSD Date Analyzed: 11/02/2014 l518h Test Code: 300.0-W Chloride 109 mg!L £300.0 0,0751 1.00 50.00 60.1 98.0 90-110 110 0.660 20 Lab Sample ID: 1410353-Q15AMSD Date Analyzed: 11102/2014 1858h Test Code: 300.0-W Chloride 88.5 mg!L £300.0 oms1 1.00 50.00 38.9 99.3 90-110 88.7 0240 20 Lab Sample ID: 1410353-009AMSD Date Analyzed: 11102/2014 2129h Test Code: 300.0-W Chloride 5 26 mg!L E300.0 0.00751 0.100 5.000 0 105 90-110 5.15 2.05 20 -Lab Sample ID: 141 0466-022AMSD Date Analyzed: II /06/20 14 035h Test Code: 300.0-W --------- Chloride 5.08 mg!L £300 0 0.00751 0.100 5000 0 102 90-110 5,08 0.115 20 Lab Sample ID: 1410353-00IBMSD Date Analyzed: ll/03/2014 l039h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.88 mg!L E353 2 0.00833 0.0100 l 000 1.03 85.1 90-110 1.86 1.28 lO Lab Sample ID: 1410353-0ilBMSD Date Analyzed: 11/03/2014 1122h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 120 mg!L E353.2 0.833 100 100.0 16.1 104 90-110 Ill 7.43 10 Lab Sample ID: 1411097-QOIDMSO Date Analyzed: 11/11/2014 ll32h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (USN) 1.04 l'Og/1. E353.2 0.00833 0.0100 1.000 0 104 90-110 1.03 0.965 10 1 -Matrix spike recovery indicates matrix interforence. The method is in control as indicated by the LCS. Rc[J<)rt Date: I l I 12120 14 Pil~ 51 of 55 All nn111y\~ f1f't)llu:nhl(' ICJ I he: CWA. SDWA. nnd RCR \ m't JIC'fformcd m accordance (Q "-l!L\(. fW(tfl~ul• Penu~'l 4.:LMJ)Iing informntion is locnted on the attached C'OC'. Confidential Bus mess. lnfonnation: This report 1s provid~d for the exclus1vc vUJ t'flttcr addressee. Priv•lc~es u,·wM.ccl\lcnt us~ of the na"1~ of'lhf'Jil c:o:mp011'f (llf.-uy member of Its stnn: C)r f\•r,raduLr~lcm of1ll1s report in comto:hOO \\Jih lhO~th."C'nl\.l.:t1JoCJtl~ ,).iomQtion or snh: of any product or process. or in conncctil:m with the re-publication o1'1his report for any purpose-otht:r thml tbr thr :i•i~\te will be grunted only lM:t l'\.U11DCt This conljlllll~ <~«<111> ltll I'C$f1'l<Wbility except for the duo p<<tbnn,Ulco of inspection and/or Nr~IHQ In P'OII fulth .,J .K"<Ot~blll! ro the rules of the trade and of science American West Analytical Laboratories UL Denison WORK ORDER Summary Work Order: 1410353 Due Date: 11/4/2014 Page I of4 Client: Client ID: Project: Comments: Sample ID 1410353-00IA 1410353-0018 1410353-00IC 1410353-002A 1410353-0028 141 0353-002C 1410353-003A 1410353-0038 141 0353-003C 1410353-004A 1410353-0048 1410353-004C 1410353-005A 1410353-0058 1410353-005C Printed: ll/4/20 14 Energy Fuels Resources, Inc. DENlOO 4th Quarter Chloroform 2014 Contact: Garrin Palmer QC Level: III WO Type: Project PA Rush. QC 3 (Summary/No chromatograms). RL of 1 ppm for Chloride and VOC and 0.1 ppm for N02/N03. Expected levels provided by client-see Jenn. J-flag what we can't meet. ElM Locus and EDD-Denison. Email Group.; Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage TW4-25_10212014 10/2112014 1252h 10/24/2014 0950h 300.0-W Aqueous ~ df· we I SEL Analyrcs: CL N02/N03-W-353.2 Rl df· no2/no3 I SELAnalytes: N03N02N 8260-W [;i'i VOCFridge Test Group: 8260-W-Custom; #of Analytes: 41 # ofSurr: 4 TW4-24_10212014 I 0/21/2014 l305h 1 0/24/2014 0950h 300.0-W Aqueous l'll df-wc I SEL Analytes: CL N02/N03-W-353.2 IV'l df· no2/no3 I SEL Atral)~es: N03N02N 8260-W ~ VOCFridge Test Group: 8260-W-Custom: # cf Am.Jiytt!.S: 4 I# cfSurr: 4 TVV4-22_10212014 10/21/2014 1313h 1 0/24/20 14 0950h 300.0-W Aqueous i'lJ df-wc I SEL Analytes: CL N02/N03-W -353.2 loti df-no2/no3 I SEL A1rolyt~~: N03N02N 8260-W f~j VOCFridge Test Gro':£.: 8260-W-Custom: #of Analytes: 4 1 # ofSurr: 4 TVV4-20_102l20l4 10/2112014 1322h 10/24/2014 0950h 300.0-W Aqueous ~l df-wc I SEL Ana(vtes: CL N02/N03-W-353.2 ~I df -no2/no3 I SEL Ar~alytes: N03N02N 8260-W 1,11 VOCFridge Test Group: 8260-W-Custom: #of Analytes: 4 1# ofSurr: 4 ~-26_10212014 10/21/2014 1328h 10/24/2014 0950h 300.0-W Aqueous f~J df·wc I SEL Analytes: CL N02/N03-W-353.2 !~I df • no2/no3 I SEL Analytes: N03N02N 8260-W ~i VOCFridge Test Group: 8260-W-Custom: #of Analytes: 4 1 # ofSurr: 4 FORLABORATORYUSEONLY[filloutonpage1]: %M 0 RT O CN O TAT O OCO HOK ___ _ HOK HOK_ _ _ _ COC Emailed ______ _ 3 3 3 3 3 WORK ORDER Summary Work Order: 1410353 Page 2 of4 Client: Energy Fuels Resources, Inc. Due Date: ll/4120 14 SampleiD Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1410353-006A MW-04_10212014 I 0/21/2014 1335h 10/24/2014 0950h 300.0-W Aqueous l\11 df-we I SEL Analytes: CL 1410353-0068 N02/N03-W-353.2 ;./ df-no2/no3 1 SEL Analytes: N03N02N 1410353-006C 8260-W ~ VOCFridge 3 Test Group: 8260-W-Custom; #of Antilytes: 4 I # ofSurr: 4 1410353-007A TW4-04_102120l4 IOI21/20141341h I 0/24/20 14 0950h 300.0-W Aqueous ~I df-wc 1 SEL Ana[ytes: CL 1410353-0078 N02/N03-W-353.2 i~l df-no2/no3 I SEL Ana{vtes: N03N02N 141 0353-007C 8260-W !\II VOCFridge Test Group: 8260-W-Custom: #of A11nfytu : 4 I # of Sun·: 4 141 0353-008A TW4-l9 _10212014 I0/21120141415h 10/24/2014 0950h 300.0-W Aqueous v df-wc I SEL Analytes: CL 1410353-0088 N02/N03-W-353.2 ~ df-no2/no3 1 SEL Analytes: N03N02N 141 0353-008C 8260-W ~ VOCFridge 3 Test Group: 8260-W-Custom; #of Arm{wes: 4 I# of SUn-: 4 1410353-009A TW4-03R_l0222014 10/22/2014 1008h 1 0/24/20 14 0950h 300.0-W Aqueous 1~1 df-wc 1 SEL Analytes: CL 1410353-0098 N02/N03-W -353.2 I'll df-no2/no3 1 SEL Analytes: N03N02N 1410353-009C 8260-W I~ VOCFridge 3 Test Group: 8260-W-Custom: # oj"AII/Jlytes: 4 I# of Surr: 4 1410353-010A TW4-03_10232104 10/23/2014 0709h 10/24/2014 0950h 300.0-W Aqueous ~ df-wc 1 SEL Analytes: CL 1410353-0108 N02/N03-W-353.2 lv-J df-no2/no3 I SEL Analytes: N03N02N 1410353-0IOC 8260-W I~ VOCFridge 3 Test Group: 8260-W-Custom: # oj A'lalj"tts: 4 I# ofSurr: 4 1410353-0IIA TW4-l2_10232014 10/23/2014 0719h I 0/24/2014 0950h 300.0-W Aqueous ~ df-wc 1 SEL Ana{vtes: CL 1410353-0118 N02/N03-W-353.2 IY.l df-no2lno3 I SELAnalytes: N03N02N 1410353-0IIC 8260-W ~ VOCFridge 3 Test Group: 8260-W-Custom: #of Ana_lytes: 4 I # o.fSurr: 4 1410353-012A TW4-28_10232014 I 0/23/20 14 0726h I 0/24/20 14 0950h 300.0-W Aqueous I~ df-wc I SEL Anal tes: CL Printed: 1114/20 14 FOR LABORATORY USE ONLY [fill out on page 1]: %M [J RT 0 CN [J TAT 0 ac o HOK ____ HOK ____ HOK._ ___ COC Emailed _______ WORK ORDER Summary WorkOrder: 1410353 Page3 of4 Client: Energy Fuels Resources, Inc. Due Date: ll/4/2014 Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Set Storage 1410353-0128 TW4-28_10232014 I 0/23/2014 0726h 10/24/2014 0950h N02/N03-W-353.2 Aqueous \{, df-no2/no3 I SELAna~vtes: N03N02N 1410353-012C 8260-W I~ I VOCFridge J Test Group: 8260-W-Custom: #of Analytes: 4 I# Q(Surr: 4 l410353-013A TW4-32_10232014 I 0/23/2014 0734h 10/24/20 14 0950h 300.0-W Aqueous r.ll df-wc I SEL Analytes: CL 1410353-0138 N02/N03-W-353.2 I~ df-no2/no3 I SEL Analytes: N03N02N 1410353-013C 8260-W ~ VOCFridge 3 Test Gmup: 8260-W-Custom; # qf Analytes: 4 I # ofSurr: 4 1410353-014A TW4-13_10232014 I 0123/2014 0740h I 0/24/20 14 0950h 300.0-W Aqueous ~ df-wc I SE:L Analytes: CL 1410353-0148 N02/N03-W-353.2 I~ I df-no2/no3 1 SE:L Ana(vtes: N03N02N 1410353-014C 8260-W ~I VOCFridge Test Group: 8260-W-Custom; li of Alla~\'11!$.' 4 I# ofSwr: 4 1410353-015A TW4-l4_10232014 I 0123/2014 0746h 10124/2014 0950h 300.0-W Aqueous i~i df-wc 1 SE:L Analytes: CL 1410353-0158 N02/N03-W -353.2 ~ df-no2/no3 I SE:L Ana~vtes: N03N02N 1410353-0 15C 8260-W ~ VOCFridge ~ Test Group: 8260-W-Custom: #of Analytes: 4 I# of Sun·: 4 1410353-016A TW4-36_10232014 1012312014 0755h 1012412014 0950h 300.0-W Aqueous I~ I df-wc I SEL Analytes: CL 1410353-0168 N02/N03-W-353.2 ~~ df-no2/no3 I SEL Analytes: N03N02N 1410353-016C 8260-W ~j VOCFridge Test Group: 8260-W-Custom: #of Analytes: 4 I# ofSurr: 4 1410353-017A TW4-27_10232014 1012312014 0802h I 0124120 14 0950h 300.0-W Aqueous ~i df-wc 1 SEL Ana(vtes: CL 1410353-0178 N02/N03-W -353.2 ':~i df-no2/no3 1 SEL Analytes: N03N02N 14!0353-017C 8260-W bZ1 VOCFridge 3 Test Group: 8260-W-Custom: #of Analyles: 4 I# ofSurr: 4 1410353-018A TW4-30_10232014 I 0123120 14 0808h 10/24/2014 0950h 300.0-W Aqueous i;fl df-wc I SEL Analytes: CL 1410353-0188 N02/N03-W-353.2 [~I df-no2/no3 1 SE:L Analytes: N03N02N Printed: ll/4/20 14 FOR LABORATORY USE ONLY [fill out on page 1): %M 0 RT 0 CN 0 TAT 0 QC[J HOK ____ HOK ____ HOK_ ___ COC Emailed _______ WORK ORDER Summary Work Order: 1410353 Page4 of4 Client: Energy Fuels Resources, Inc. Due Date: ll/4/20 14 Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1410353-0 18C TW4-30_10232014 10/23/2014 0808h 10/24/2014 0950h 8260-W Aqueous ~ VOCFridge Test Group: 8260-W-Cuslonr; # o/AIIalyles: 4 I # ofSurr: 4 1410353-019A TW4-65_10232014 10/23/2014 0719h 10/24/2014 0950h 300.0-W Aqueous l~i df-we 1 SEL Ana~VIes: CL 1410353-019B N02/N03-W-353.2 ~ df-no2/no3 1 SEL Analytes: N03N02N 1410353-019C 8260-W ~ VOCFridge 3 Test GI'OIIp: 8260-W-Custonr; #of. l410353-020A TW4-60_10232014 l 0/23/20 14 0830h l 0/24/2014 0950h 300.0-W Aqueous ~I df-we I SEL Analytes: CL 1410353-0208 N02/N03-W-353.2 1~1 df-no2/no3 1 SEL Anofytes: N03N02N 1410353-020C 8260-W ~ VOCFridge Test Group: 8260-W-Custom: #of Analytes: 4 I # ofSurr: 4 1410353-021A Trip Blank 10/21/2014 l 0/24/20 14 0950h 8260-W Aqueous ~I VOCFridge 3 Printed: l 114/2014 FOR LABORATORY USE ONLY [fill out on page 1]: %M 0 RT 0 CN 0 TAT U QC 0 HOK ___ _ HOK ___ _ HOK.... _ _ _ COC Emaifed ______ _ American West Analytical Laboratories 463 W. 3600 S. Salt Lake City, UT 84115 Phone # (801) 263-8686 Toll Free# (888) 263-8686 CHAIN OF CUSTODY All analysis will b43 conducted using NELAP accredited methods and all data will be repor1ed using AWAL's standard analyte lists and reporting limits (PQL) unless specifically requested otherwise on this Chain of Custody and/or attached documentation. \L\ \O~S5 AWAL Lab Sample Set# Page 1 of 2 signed reports will be email ad by 5;00 pm on -' L._.~ Fax# (801)263-8687 Email awal@awal-labs.com I QCLevel: I TumAroundTime: 'unlessotherarrangementshavebeenmade,IDlia Om:· --~ -W'M/J.awal-labs.com 3 Standard the day they are duo. - ~·d1 ~t ·'Y' • .:.r'~~;:~ .-! Client: Energy Fuels Resources, Inc, )( Include EDD: ~-· .;!i!!_I@;,~~!YW.~.tJ~.Y-"""11 5 1 1 LOCUS UPLOAD , _ ~"" • ,. Address: 642 S. Hwy. 9 EXCEL .,._, '""', . -, , ''W· --.,.-ca ..... '!ro::_ ·' .• -~ --• Blanding, UT 84511 Field Filtered For: 1 -~--~~,;---, ;· -,~~·~r.;. - Contact: Garrln Palmer 1-------------U -~ i·~lf;~\ , ForCompllanceWith: -~--: r •- Phone#: (435) 67S-22 21 CeQ#: D NELAP 'S TcftilpJm,....-~-·o; gpiiDler@energyfuelS.com; KWe1nel@energy.fuelS.com; 0 RCRA • .;-_ _ __ ~ -~-r • Email: dtnrk@Jcnergyfuels.com D CWA _. ~v..:'~'?~~ ~ D SDWA (~'.~ , • Project Name: 4th Quarter Chloroform 2014 0 ELAP 1 A2LA y' ~_: ~~ '0 ~ · :, ~ 0 0 NLLAP , -_I• Project#: "! 0 D Non-Compliance S~: . . P.t~ . -i;l o ,.,_ D Other. • ~ v, · ~ ,(1 PO#: "> "> 0 <', "'"'~·'"' '"• ~ 1:$ -...:.. .._ a I c~ • ~ !"i'QP'r • T H ll"d :g ::-0') 0 \0 y !' '. ;: Sampler Name: anner o 1 ay 2 " 0 o iJ , 'II , '-' r---....:--....:.--==================;=====:::;i==i===~ § ~ ;.; ~ ~ Known Hazards ~ ll~:-1 ~~ • ,~ , Date Time u c. N" ~ Cj & ~~ . , • oEo-o f.l •• SampleiD: Sampled Sampled .._ cill :.: tJ :> Sample Comments . _ ·,, :-.~·--'I I TW4-25_10212014 10/21/14 1252 5 W X x x ~ ~ ••. ·, :<-:·~~-; s t TW4-24 10212014 10/21/14 1305 5 w x x x ~--" "' ·•r -.....,.,...,.w....: ' -• I TW4-22_10212014 10/21/14 1313 5 w X X X ,· •' ~~On·~··(~·--:-: ~.-- 1 TW4-20 10212014 10/21/14 1322 5 w X X X .: • .!c.~.. ·-.·~. ~ -~ . .. -_ --2• ~1-Dn'OUiorP '· • i 1'4\V-26 10212014 10/21/14 1328 5 W X X X .• 'I' ,., ~ --~ -•. ! MW-04~10212014 10/21/14 1335 5 w X X X t .~~~:·~~-~ -·IDT.· . .--· '"" ,,, ·" ~"'"" -f TW4-04_10212014 10/21/14 1341 5 w X X X • • , • ·'· ~' • -:" '~ I TW4-19_10212014 10/21/14 1415 5 w X X X ~·l\..·:~:·~t€J.L 5 E I TW4-03R_10222014 10/22/14 1008 5 w X X X ~--ilil·e~:sbm~~ , '· ' ~ cO.C ··~ 0 TW4-03_10232104 10/23/14 709 5 w X X X ~7 ---~~-.' f., TW4-12_10232014 10/23/14 719 5 w X X X -• .. l TW4-28_10232014 10/23/14 726 5 w X X X ~·f.·' .. ,'.; ~';~-·. V.· { • _,---I . .! ~ -~ • .If'. ~ TW4-32_10232014 10/23/14 734 p w X X X ·~ -.. ' ~ i:~br. ~ g'LA--"'tolz3/t~ ==t>·r: _ ...... Date: Speciallnstructions: Pllh!Nom"' &-.c.. ..... ;... "P-l ~ ome: I ·zoo f'!liltf'bmal ----Tfme: ROil~trr. ate: R.-ro<l-.y; ,_,...-pate: See the Analytical Scope of Work for Reporting Limits and VOO Sl!in<>l~ _ ~~..w. __.,-arui.lylc Jist. T1me; ~ rnme: PrinlName: arill.~ ~ctinquished by: !late: __..-<oelllYOCI by: ate: Signature ~ ISJgnoMo Print Name: / ~o: PJtnlNa=" ......,_ f' ,., " lme: ::L.":'""I>(: / Date: ~~:~u:!~y IQ~A i.J.O~Lt.A ) I'''~"" 10/2t.\, t'-{ P!lni Name: ./ Ttmo p,lnlN J{)N\,_l~¥:,f"u.l)./'"{\ !'"""" q ~.&!J 0 , bB Jz~/ Jy American West Analytical Laboratories 463 W. 3600 S, Salt Lake City, UT 84115 Phone# (801) 263-11686 Toll Free# (888) 263-BB86 L~~ Fax# (801) 263-8687 Email awal@awal-labs.com www.awa~labs.com Client Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Contact Garrin Palmer Phone#: (4351 678-2221 Cell#: iiJUlLIIItJfbili•-rzyluili:COCnl XWolno¢cwe~rofuC$Lc:o-m:: Email: ct~•no!'I!!~Mt...oom Project Name: 4th Quarter Chloroform 2014 Project#: PO#: Sam pier Name: Tanner Holliday Date Sampi!!ID: Ssmplecd I T\V'I-13_10232014 10/23/14 ! 'TW'I-14.10232014 10/23/14 1 TW4-36_10232014 10/23/14 I TW'I-2'7_10232014 10/23/14 ; TW4-3o.l0232014 10/23/14 ; 'TW4-6S.10232014 10/23/14 r TW4-60_10232014 10/23/14 ! Tdp Blank 10/21/14 i Tmnp Blank ~ I I I __ .,._ ~ ~ llol•'t o I ?.Jl~<J s;,,.o,r.- (;...c,_;r r ~ "'-i?"'"'""'-""-(.,..o' l'lmoi rrvrJ Prinl Ndmc.: :-=....-...-:""'" Pn.t-. rr- ll*-"Y· ate: sunohlno flmo: l't!r.tlloiM' Ro-'11' Oato: ~-fime: """""""" I Time Samoled 740 746 755 802 808 719 830 eceived by: Signalure _..._ CHAIN OF CUSTODY All analysis will be conducted using NELAP accr9dlled methods end all daiE!I wWI be reported using AWAL's slandard analyte lists •nd reporting llmil5 (POL) Unle~ spe&ifie&lly requested otherwlsa on this Chain of Custody and/Cf allached documBnlltion. QC Level: I Turn Around Time: Unless other arrangements have been made, signed reports .....til be emailed by 6:00 pm on 3 Standard lho day lhoy oro duo. ~ lncludeEDD: LOCUS uPLOAD EXCEL Field Filtered For. I for Compliance Wtth: I 0 NELAP 0 RCRA 0 CWA 0 SDWA 0 ELAP/A2lA 0 0 NLLAP "' d 0 Non-Compliance [;j 0 D Olher. 0) U' ~ :S 12. k 0 <') 0 "' :§ ~ 0 0 " § :; 1': ~ (!?.. Known Hazards "' m ~ :t. t1 c. & '0 ~ ~ 0 0 Sample Comments .. "' ~ 5 w X X X 5 .. X X X 5 w X X X 5 .. X X X 5 w X X X 5 w X X X 3 ... X X X , w X I w bs.te: Special Instructions: 1me: IL-l \03S3 A'/lll.k Lab Sample Set# Page 2 of r-u.~'O·?·': .= > I ~~ ;l;ll~I~Me O.fl~\ ._,-,._ -:w.... "'' --. ... ~w~--::vec.. ex -~Gt-·:·· ~~.---~-- "' r-&.6 J~·~-1 , ~~ ··~~~~"' jj '. &· .. · .. -~ .. ~ \-. -· .,._ !:':'. ~~v~,. ··:p . ' -· ~ t' .. y -.~-"!~· .. ~·· .~· ~ .(5¥10~~ .. I i ~~ .~ ;n-.' .---~~~ 1: . I' 1)"' ·'-"~ . ..,. .. --~ ... ~.,. -" -· !'• J ' ~ 1-· ... .,...._ ,. "',· 1. 'N HAc ': '=. ~ ~ .~' ~9~0Uli)li~ I -~ .,--r.·: ·: -J~ ·~ . ·-:~-®. !-·t ~· ~Sam,.. --,., J; ..;~ ~~; .. -"".. . -·--' • ~: ... S.-· ®' . I y • ' ,., ...•. lifo• =· --~ ~ ., -- ' ~~~w ··->' y: ,. -.JI ••' . . . " :~ =·l>y, ""'"' See the Analytical Scope of Work for Reporting Limits and VOC analyte list. 1\mt: Ptjl'l"'r.t..'\mc Received y: bale: Sk;!nalure I me: ................ ~ I I kmlvod b~ J... )o A,(\ r.t..n SiQnsture AA l . ""' -l0f2L/J l'-l """ ....... r.1 p .11'\ i. c::;,o '. ~'{' U-~ TIJDO q .:.9() Preservation Check Sheet Lab Sample Set#: 141353 ~~or~ *'.:002t· ~ i'&Q;.4~ ~oas-.c:: g:.oa& ... r-oov q _._ :l'!o09~ =:i:£Ji oJ ;~i., '~:0~12'<.1 ·-~~ "'6~!10::' ·~i~-~.i:Q16~r ~-~ l. ~" -~~ ,...--~~ ·_ .. ,;;008~ ~~ II •.__ I• ' I ~-·-l r,... , ........ ~~~ • N02/N03: pH <2 H2S04 YES YES YES YES YES YES YES YES YES YES YES YES YES YES YES YES - NOJN03: pH <2 H2S04 L---~----~-----L----~----~--~----~-----L----~----~--~~--~-----L----~----~--~ TabH Quality Assurance and Data Validation Tables H-1 Field Data Q;VQC Evaluation Volume Location Casing Volume 2x Casing Volume Pumped Volume Check Coudnctivity, RPb pB RPD Temp RPD Redox Potcnfiill RPD Turbidity RPl> Piezometer 1 --2130 NC 8.40 NC 15.33 NC 150 NC 1.3 NC Piezometer 2 --816 NC 6.94 NC 15.43 NC 236 NC ;s~' NC Piezometer 3 --2743 NC 11.56 NC 15.29 NC 88 NC -·~ z:. NC TWN-1 34.30 68.60 88.00 OK 845.0 852.0 0.82 6.94 6.94 0.00 15.00 15 .00 0.00 227 I 226 0.44 ~QI -:n-3.92 TWN-2 NA Continuously Pumped Well 3438 NC 6.30 NC 16.70 NC 291 NC 5,8; ·~ NC TWN-3 37.88 75.76 47.66 Pumped Dry 2271.0 2283.0 0.53 6.83 6.81 0.29 14.48 14.58 0.69 NM NC NM NC TWN-4 47.93 95.86 121.00 OK 963.0 971.0 0.83 6.73 6.73 0.00 14.69 14.70 0.07 223 I 222 0.45 1!1.3 _ I) t:,t_;; 1.75 TWN-7 12.28 24.56 16.50 Pumped Dry 1287.0 1281.0 0.47 7.38 7.35 0.41 15.47 15.45 0.13 NM NC NM NC TWN-18 55.83 111.66 132.00 OK 2191.0 2180.0 0.50 6.46 6.47 0.15 14.51 14.50 0.07 239 I 238 0.42 19~0 u _14.tt. 7.41 TW4-22 NA Continuously pumped well 5992 NC 6.40 NC 15.55 NC 174 NC 3.0 NC TW4-24 NA Continuously pump~:d well 8998 NC 6.35 NC 15.28 NC 182 NC 1.5 NC TW4-25 NA C.<lnlinuously.pumped well 2614 NC 6.35 NC 15.95 NC 290 NC 0 NC NC = Not Calculated TWN-2, TW4-22, TW4-24, and TW4-25 are continuously pumping wells. NM = Not Measured. The QAP does not require the measurement of redox potential or turbidity in wells that were purged to dryness. H-2: Holding Time Evaluation Allowed Hold Time Hold Time Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) (Days) Check PIEZ-01 Chloride 10/8/2014 10113/2014 5 28 OK PIEZ-01 Nitrate/Nitrite (as N) 10/8/2014 10110/2014 2 28 OK PIEZ-02 Chloride 10/8/2014 10113/2014 5 28 OK PIEZ-02 Nitrate/Nitrite (as N) 10/8/2014 10/20/2014 12 28 OK PIEZ-03 Chloride 10/8/2014 10/13/2014 5 28 OK PIEZ-03 Nitrate/Nitrite (as N) 10/8/2014 10110/2014 2 28 OK TWN-01 Chloride 10/8/2014 10113/2014 5 28 OK TWN-01 Nitrate/Nitrite (as N) 10/8/2014 10110/2014 2 28 OK TWN-02 Chloride 10/8/2014 10113/2014 5 28 OK TWN-02 Nitrate/Nitrite (as N) 10/8/2014 10110/2014 2 28 OK TWN-03 Chloride 10/9/2014 10113/2014 4 28 OK TWN-03 Nitrate/Nitrite (as N) 10/9/2014 10/10/2014 1 28 OK TWN-04 Chloride 10/8/2014 10/13/2014 5 28 OK TWN-04 Nitrate/Nitrite (as N) 10/8/2014 10110/2014 2 28 OK TWN-07 Chloride 10/9/2014 10/13/2014 4 28 OK TWN-07 Nitrate/Nitrite (as N) 10/9/2014 10110/2014 1 28 OK TWN-07R Chloride 10/8/2014 10/23/2014 15 28 OK TWN-07R Nitrate/Nitrite (as N) 10/8/2014 10110/2014 2 28 OK TWN-18 Chloride 10/8/2014 10113/2014 5 28 OK TWN-18 Nitrate/Nitrite (as N) 10/8/2014 10110/2014 2 28 OK TW4-22 Chloride 10/21/2014 11/2/2014 12 28 OK TW4-22 Nitrate/Nitrite (as N) 10/2112014 11/3/2014 13 28 OK TW4-24 Chloride 10/21/2014 11/2/2014 12 28 OK TW4-24 Nitrate/Nitrite (as N) 10/21/2014 11/3/2014 13 28 OK TW4-25 Chloride 10/21/2014 11/5/2014 15 28 OK TW4-25 Nitrate/Nitrite (as N) 10/21/2014 11/3/2014 13 28 OK TW4-60 Chloride 10/23/2014 11/2/2014 10 28 OK TW4-60 Nitrate/Nitrite (as N) 10/23/2014 11/3/2014 11 28 OK TWN-60 Chloride 10/8/2014 10/23/2014 15 28 OK TWN-60 Nitrate/Nitrite (as N) 10/8/2014 10/10/2014 2 28 OK TWN-65 Chloride 10/8/2014 10/13/2014 5 28 OK TWN-65 Nitrate/Nitrite (as N) 10/8/2014 10/10/2014 2 28 OK H-3: Analytical Method Check .Pru-abtt~ ' Method Method Used by.I;.ab ~ Nitrate E353.1 or E353.2 E353.2 A4500-Cl B or A4500-Cl E Chloride or E300.0 A4500-Cl-E Both Nitrate and Chloride were analyzed with the correct analytical method. H4R -cpor1m2 lffilt ec L' . Ch k Required Lab Reporting Reporting Dilution Location Analyte Limit Units ,Qualifier Limit RLCheck Factor PIEZ-01 Chloride 5 mg/L I OK 1 PIEZ-01 Nitrate/Nitrite (as N) O.I mg/L 0.1 OK 10 PIEZ-02 Chloride 5 mg!L 1 OK 1 PIEZ-02 Nitrate/Nitrite (as N) 0.01 mg/L 0.1 OK 1 PIEZ-03 Chloride 5 mg!L 1 OK I PIEZ-03 Nitrate/Nitrite Cas N) 0.01 mg/L O.I OK 1 TWN-01 Chloride 5 mg/L I OK 1 TWN-01 Nitrate/Nitrite (as N) 0.01 mg/L 0.1 OK 1 TWN-02 Chloride 5 mg!L 1 OK 1 TWN-02 Nitrate/Nitrite (as N) 1 mg/L O.I OK 100 TWN-03 Chloride 50 mg!L I OK 10 TWN-03 Nitrate/Nitrite (as N) I mg/L 0.1 OK 100 TWN-04 Chloride 5 mg/L I OK 1 TWN-04 Nitrate/Nitrite (as N) 0.01 mg/L 0.1 OK 1 TWN-07 Chloride 5 mg/L 1 OK I TWN-07 Nitrate/Nitrite (as N) 0.01 mg!L O.I OK 1 TWN-07R Chloride 1 mg/L u I OK I TWN-07R Nitrate/Nitrite (as N) 0.1 mg/L u O.I OK 1 TWN-18 Chloride 5 mg/L 1 OK 1 TWN-18 Nitrate/Nitrite (as N) 0.01 mg/L O.I OK 1 TW4-22 Chloride 100 mg!L 1 OK 100 TW4-22 Nitrate/Nitrite (as N) 10 mg/L 0.1 OK 100 TW4-24 Chloride 100 mg/L 1 OK 100 TW4-24 Nitrate/Nitrite (as N) 10 mg/L 0.1 OK 100 TW4-25 Chloride 10 mg/L 1 OK IO TW4-25 Nitrate/Nitrite (as N) 0.1 mg/L 0.1 OK 1 TW4-60 Chloride 1 mg/L u 1 OK I TW4-60 Nitrate/Nitrite (as N) O.I mg/L u O.I OK 1 TWN-60 Chloride 1 mg/L u 1 OK I TWN-60 Nitrate/Nitrite (as N) O.I mg/L u 0.1 OK I TWN-65 Chloride 5 mg/L I OK 1 TWN-65 Nitrate/Nitrite (as N) 0.01 mg!L O.I OK I U =Value was reported by the laboratory as nondetect. H-5 QA/QC Evaluation for Sample Duplicates CZonstih.len't I ~~l8' TW!N=65 ~ %1U>D Chloride 74.8 72.3 3.40 Nitrogen 1.47 1.47 0.00 H-6 QC Control Limits for Analysis and Blanks Method Blank Detections All Method Blanks for the quarter were non-detect. MatriK Soike % Recovery C --------t:--·-........... 1 ........ ··~~·· Lab Report Lab Sample ID Well Analyte MS %REC 1410138 1410137-003CMS N/A Chloride 1410138 1410138-001AMS TWN-07 Chloride 1410353 1410353-00lBMS TW4-25 Nitrate * -Recovery was not calculated because the analyte of the sample was greater than 4 times the spike amount N/ A -QC was not performed on an EFRI sample. NC-Not calculated Laboratory Control Sample All Laboratory Control Samples were within acceptance limits for the quarter. 84.1 86.3 82.7 REC MSD %REC Range RPD 76.1 90-110 1.22 84.1 90-110 1.52 85.1 90-110 1.28 H7R . T E 1 -cce1p1 empcrt~ll!rc va uatiOn Sample BatCh W~IIS iri' Batcb niupi!r~wre Piezometer 1, Piezometer 2, Piezometer 3, TWN-1, TWN-2, 1410138 TWN-3, TWN-4, TWN-7, TWN-07R, TWN-18, TWN-60, 4.2 "C TWN-65 1410353 TW4-22, TW4-24, TW4-25, TW4-60 1.1 "C H-8 Rinsate Evaluation All rinsate and DI blank samples were non-detect for the quarter. Tab I Kriged Current Quarter Isoconcentration Maps NS = not sampled; ND = not detected ...._ 10 kriged nitrate isocon and label MW-4 perched monitoring well showing e 5.1 concentration in mg/L TW4-_1 temporary perched monitoring well 0 6.3 showing concentration in mg/L TWN-1 temporary perched nitrate monitoring ~ 1.5 well showing concentration in mg/L PIEZ-1 perched piezometer showing ~ 5.8 concentration in mg/L TW4-35 temporary perched monitoring well ~ 0 35 installed May, 2014 showing • concentration in mg/L NOTE: MW-4, MW-26, TW4-4, TW4-19, and TW4-20 are chloroform pumping wells; TW4-22, TW4-24, TW4-25, and TWN-2 are nitrate pumping wells HYDRO GEO CHEM,INC. KRIGED 4th QUARTER, 2014 NITRATE {mg/L) {NITRATE + NITRITE AS N) WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H:f718000/feb15/nitrate/Unt1214.srf I I -1 NS =not sampled; ND =not detected ...._ 100 MW-4 .42 TW4-1 0 39 TWN-1 0 28 PIEZ-1 ~58 TW4·36 ~67 kriged chloride isocon and label perched monitoring well showing concentration in mg/L temporary perched monitoring well showing concentration in mg/L temporary perched nitrate monitoring well showing concentration in mg/L perched piezometer showing concentration in mg/L temporary perched monitoring well installed May, 2014 showing concentration in mg/L 1. mile NOTE: MW-4, MW-26, TW4-4, TW4-19, and TW4-20 are chloroform pumping wells; TW4-22, TW4-24, TW4-25, and TWN-2 are nitrate pumping wells HYDRO GEO CHEM,INC. KRIGED 4th QUARTER, 2014 CHLORIDE (mg/L) WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H:/718000/ffeb15/chloride/Ucl1214.srf I I -2 TabJ Analyte Concentrations Over Time Piezometer 1 Date Nitrate (mg/1) Chloride (mg/1) 2/19/2009 6.8 NA 7/14/2009 6.8 60 9/22/2009 7.3 78 10/27/2009 7.4 61 6/2/2010 7.2 52 7/19/2010 6.8 52 12/10/2010 6.5 60 1/31/2011 7 60 4/25/2011 6.8 58 7/25/2011 7 53 10/19/2011 6.6 55 1/11/2012 7.1 78 4/20/2012 6.6 58 7/27/2012 7.2 56 10/17/2012 7.66 55 2/18/2013 8.11 56.7 4/24/2013 8.88 53.3 8/28/2013 7.83 55.1 10/16/2013 6.68 54.1 1/13/2014 6.79 56.2 5/7/2014 7.57 52.1 8/6/2014 5.1 55 10/8/2014 5.75 57.6 Piezometer 2 Date Nitrate (mg/1) Chloride (mg/1) 2/19/2009 0.5 NA 7/14/2009 0.5 7 9/22/2009 0.5 17 10/27/2009 0.6 7 6/2/2010 0.6 8 7/19/2010 0.6 8 12/10/2010 0.2 6 1/31/2011 0.3 9 4/25/2011 0.3 8 7/25/2011 0.1 9 10/19/2011 0.1 8 1/11/2012 0.1 9 4/20/2012 0.2 8 7/27/2012 0.2 9 10/17/2012 0.192 9.5 2/19/2013 0.218 9.67 4/24/2013 0.172 10.3 8/28/2013 0.198 9.66 10/16/2013 0.364 9.22 1/13/2014 0.169 11.4 5/7/2014 0.736 11.4 8/6/2014 0.8 12 10/8/2014 0.755 12.2 Piezometer 3 Date Nitrate (mg/1) Chloride (mg/1) 2/19/2009 0.7 NA 7/14/2009 0.8 12 9/22/2009 0.8 24 10/27/2009 1.2 19 3/24/2010 1.7 116 6/2/2010 1.6 36 7/19/2010 1.6 35 12/10/2010 1.8 25 1/31/2011 1.8 40 4/25/2011 1.7 35 7/25/2011 1.8 61 10/19/2011 1.7 12 1/11/2012 1.8 20 4/20/2012 1.7 53 7/27/2012 1.8 21 10/17/2012 2.75 20.1 2/19/2013 1.85 21 4/24/2013 1.83 21.2 8/28/2013 1.81 22.4 10/16/2013 1.80 23 .5 1/13/2014 1.70 26.0 5/7/2014 1.79 23.9 8/6/2014 1.7 26 10/8/2014 1.74 28.3 TWN-1 Date Nitrate (mg/1) Chloride (mg/1) 2/6/2009 0.7 19 7/21/2009 0.4 17 9/21/2009 0.4 19 10/28/2009 0.5 18 3/17/2010 0.5 17 5/26/2010 0.6 20 9/27/2010 0.6 19 12/7/2010 0.6 14 1/26/2011 0.5 17 4/20/2011 0.5 19 7/26/2011 0.5 14 10/17/2011 0.5 10 1/9/2012 0.6 15 4/18/2012 0.6 17 7/24/2012 0.6 17 10/15/2012 0.432 17.5 2/18/2013 0.681 17.6 4/23/2013 0.84 17.4 8/27/2013 1.24 24.1 10/16/2013 1.61 26.8 1/14/2014 1.47 29.2 5/6/2014 1.63 31.1 8/5/2014 1.7 28 10/8/2014 1.46 27.6 TWN-2 Date Nitrate (mg/1) Chloride (mg/1) 2/6/2009 25.4 29 7/21/2009 25 25 9/21/2009 22.6 17 11/2/2009 20.8 55 3/24/2010 62.1 85 6/2/2010 69 97 9/29/2010 69 104 12/9/2010 48 93 2/1/2011 43 93 4/28/2011 40 85 7/28/2011 33 74 10/20/2011 33 76 1/12/2012 31 86 4/20/2012 48 103 7/31/2012 54 93 10/17/2012 22.1 79 2/19/2013 57.3 80.5 4/24/2013 57.7 82.1 8/27/2013 80 75.9 10/16/2013 111 70.4 1/13/2014 42.6 72.4 5/7/2014 44.7 84.9 8/6/2014 42 80 10/8/2014 70.6 81 TWN-3 Date Nitrate (mg/1) Chloride (mg/1) 2/6/2009 23.6 96 7/21/2009 25.3 96 9/21/2009 27.1 99 11/2/2009 29 106 3/25/2010 25.3 111 6/3/2010 26 118 7/15/2010 27 106 12/10/2010 24 117 2/1/2011 24 138 4/28/2011 26 128 7/29/2011 25 134 10/20/2011 25 129 1/12/2012 25 143 4/20/2012 24 152 7/31/2012 27 158 10/17/2012 12.1 149 2/19/2013 22.2 157 4/24/2013 27.2 158 8/28/2013 20.9 171 10/17/2013 23.5 163 1/15/2014 19.6 160 5/7/2014 23.6 168 8/6/2014 19.5 174 10/9/2014 19.1 153 TWN-4 Date Nitrate (mg/1) Chloride (mg/1) 2/6/2009 1 13 7/21/2009 0.05 12 9/21/2009 0.4 13 10/28/2009 0.4 11 3/16/2010 0.9 22 5/27/2010 1.0 22 9/27/2010 0.9 19 12/8/2010 1 21 1/25/2011 0.9 21 4/20/2011 0.9 21 7/26/2011 1.1 35 10/18/2011 0.9 20 1/9/2012 0.9 20 4/18/2012 1.1 24 7/25/2012 1.4 25 10/15/2012 1.45 26.4 2/18/2013 1.51 25.3 4/23/2013 1.63 24.4 8/27/2013 1.58 27.2 10/16/2013 1.69 29.4 1/14/2014 1.41 28.4 5/6/2014 1.55 29.6 8/5/2014 2.0 28 10/8/2014 1.44 30.7 TWN-7 Date Nitrate (mg/1) Chloride (mg/1) 8/25/2009 ND 11 9/21/2009 ND 7 11/10/2009 0.1 7 3/17/2010 0.8 6 5/28/2010 1.2 6 7/14/2010 1.6 7 12/10/2010 1 4 1/27/2011 1.3 6 4/21/2011 1.7 6 7/29/2011 0.7 5 10/19/2011 2.2 6 1/11/2012 2.3 5 4/20/2012 1.2 6 7/26/2012 0.9 6 10/16/2012 0.641 5.67 2/19/2013 0.591 5.68 4/24/2013 1.16 5.88 8/28/2013 0.835 6.96 10/16/2013 0.986 5.70 1/15/2014 0.882 5.75 5/7/2014 0.564 5.26 8/6/2014 0.9 6 10/9/2014 0.968 5.93 TWN-18 Date Nitrate (mg/1) Chloride (mg/1) 11/2/2009 1.3 57 3/17/2010 1.6 42 6/1/2010 1.8 63 9/27/2010 1.8 64 12/9/2010 1.6 59 1/27/2011 1.4 61 4/26/2011 1.8 67 7/28/2011 1.8 65 10/18/2011 1.9 60 1/10/2012 1.9 64 4/19/2012 2.1 64 7/26/2012 2.3 67 10/16/2012 1.95 67.5 2/18/2013 2.27 68.7 4/23/2013 2.32 64.3 8/27/2013 2.04 70.4 10/16/2013 2.15 67.3 1/14/2014 2.33 68.4 5/6/2014 2.18 76.5 8/5/2014 1.8 70 10/8/2014 1.47 74.8 TW4-19 Date Nitrate (mg/1) Date Chloride (mg/1) 7/22/2002 42.80 12/7/2005 81 9/12/2002 47.60 3/9/2006 86 3/28/2003 61.40 7/20/2006 123 6/23/2003 11.40 11/9/2006 134 7/15/2003 6.80 2/28/2007 133 8/15/2003 4.00 8/15/2007 129 9/12/2003 5.70 10/10/2007 132 9/25/2003 9.20 3/26/2008 131 10/29/2003 7.70 6/25/2008 128 11/9/2003 4.80 9/10/2008 113 8/16/2004 9.91 10/15/2008 124 9/17/2004 4.50 3/4/2009 127 3/16/2005 5.30 6/23/2009 132 6/7/2005 5.70 9/14/2009 43 8/31/2005 4.60 12/14/2009 124 12/1/2005 0.10 2/17/2010 144 3/9/2006 4.00 6/9/2010 132 6/14/2006 5.20 8/16/2010 142 7/20/2006 4.30 10/11/2010 146 11/9/2006 4.60 2/17/2011 135 2/28/2007 4.00 6/7/2011 148 8/15/2007 4.10 8/17/2011 148 10/10/2007 4.00 11/17/2011 148 3/26/2008 2.20 1/23/2012 138 6/25/2008 2.81 6/6/2012 149 9/10/2008 36.20 9/5/2012 149 10/15/2008 47.80 10/3/2012 150 3/4/2009 3.20 2/11/2013 164 6/23/2009 2.40 6/5/2013 148 9/14/2009 0.10 9/3/2013 179 12/14/2009 26.70 10/29/2013 206 2/17/2010 2.00 1/27/2014 134 6/9/2010 4.40 5/19/2014 152 8/16/2010 5.90 8/11/2014 140 10/11/2010 2.70 10/21/2014 130 2/17/2011 17.00 6/7/2011 12.00 8/17/2011 3.00 11/17/2011 5.00 1/23/2012 0.60 6/6/2012 2.40 9/5/2012 2.50 10/3/2012 4.10 2/11/2013 7.99 6/5/2013 2.95 9/3/2013 17.60 10/29/2013 4.70 1/27/2014 1.62 5/19/2014 1.34 8/11/2014 1.60 10/21/2014 4.72 The sampling program for TW4-19 was updated in the fourth quarter of 2005 to include analysis for chloride as well as nitrate. This change accounts for the different number of data points represented above. TW4-21 Date Nitrate (mg/1) Date Chloride (mg/1) 5/25/2005 14.6 12/7/2005 353 8/31/2005 10.1 3/9/2006 347 11/30/2005 9.6 7/20/2006 357 3/9/2006 8.5 11/8/2006 296 6/14/2006 10.2 2/28/2007 306 7/20/2006 8.9 6/27/2007 327 11/8/2006 8.7 8/15/2007 300 2/28/2007 8.7 10/10/2007 288 6/27/2007 8.6 3/26/2008 331 8/15/2007 8.6 6/25/2008 271 10/10/2007 8.3 9/10/2008 244 3/26/2008 14.3 10/15/2008 284 6/25/2008 8.8 3/11/2009 279 9/10/2008 7.6 6/24/2009 291 10/15/2008 8.0 9/15/2009 281 3/11/2009 8.3 12/22/2009 256 6/24/2009 8.1 2/25/2010 228 9/15/2009 9.2 6/10/2010 266 12/22/2009 8.4 8/12/2010 278 2/25/2010 8.4 10/13/2010 210 6/10/2010 12.0 2/22/2011 303 8/12/2010 14.0 6/1/2011 297 10/13/2010 7.0 8/17/2011 287 2/22/2011 9.0 11/16/2011 276 6/1/2011 13.0 1/19/2012 228 8/17/2011 14.0 6/13/2012 285 11/16/2011 13.0 9/13/2012 142 1/19/2012 15.0 10/4/2012 270 6/13/2012 11.0 2/13/2013 221 9/13/2012 13.0 6/18/2013 243 10/4/2012 14.0 9/12/2013 207 2/13/2013 11.8 11/13/2013 206 6/18/2013 13.8 2/5/2014 200 9/12/2013 10.3 5/22/2014 243 11/13/2013 9.0 8/27/2014 230 2/5/2014 11.4 10/29/2014 252 5/22/2014 11.5 8/27/2014 7.1 10/29/2014 10.0 The sampling program for TW4-21 was updated in the fourth quarter of 2005 to include analysis for chloride as well as nitrate. This change accounts for the different number of data points represented above. TW4-22 Date Nitrate (mg/1) Chloride (mg/1) 2/28/2007 20.9 347 6/27/2007 19.3 273 8/15/2007 19.3 259 10/10/2007 18.8 238 3/26/2008 39.1 519 6/25/2008 41.9 271 9/10/2008 38.7 524 10/15/2008 36.3 539 3/11/2009 20.7 177 6/24/2009 20.6 177 9/15/2009 40.3 391 12/29/2009 17.8 175 3/3/2010 36.6 427 6/15/2010 19 134 8/12/2010 18 127 8/24/2010 15 130 10/13/2010 16 134 2/23/2011 18 114 6/1/2011 17 138 8/17/2011 15 120 11/16/2011 19 174 1/19/2012 14 36 6/13/2012 12.8 35 9/12/2012 7 121 10/4/2012 14 130 2/11/2013 58 635 6/5/2013 50.2 586 9/3/2013 29.7 487 10/29/2013 45.2 501 1/27/2014 54.6 598 5/19/2014 47.2 614 8/11/2014 41.5 540 10/21/2014 54.9 596 TW4-24 Date Nitrate (mg/1) Chloride (mg/1) 6/27/2007 26.1 770 8/15/2007 29 791 10/10/2007 24.7 692 3/26/2008 24.4 740 6/25/2008 45.3 834 9/10/2008 38.4 1180 10/15/2008 44.6 1130 3/4/2009 30.5 1010 6/24/2009 30.4 759 9/15/2009 30.7 618 12/17/2009 28.3 1080 2/25/2010 33.1 896 6/9/2010 30 639 8/11/2010 32 556 8/24/2010 31 587 10/6/2010 31 522 2/17/2011 31 1100 5/26/2011 35 1110 8/17/2011 34 967 11/16/2011 35 608 1/18/2012 37 373 6/6/2012 37 355 8/30/2012 37 489 10/3/2012 38 405 2/11/2013 35.9 1260 6/5/2013 23 .7 916 9/3/2013 32.6 998 10/29/2013 34.6 1030 1/27/2014 31.6 809 5/19/2014 35 1020 8/11/2014 31.5 1150 10/21/2014 35.7 1050 TW4-25 Date Nitrate (mg/1) Chloride (mg/1) 6/27/2007 17.1 395 8/15/2007 16.7 382 10/10/2007 17 356 3/26/2008 18.7 374 6/25/2008 22.1 344 9/10/2008 18.8 333 10/15/2008 21.3 366 3/4/2009 15.3 332 6/24/2009 15.3 328 9/15/2009 3.3 328 12/16/2009 14.2 371 2/23/2010 14.4 296 6/8/2010 16 306 8/10/2010 14 250 10/5/2010 15 312 2/16/2011 15 315 5/25/2011 16 321 8/16/2011 16 276 11/15/2011 16 294 1/18/2012 16 304 5/31/2012 16 287 9/11/2012 17 334 10/3/2012 17 338 2/11/2013 9.04 190 6/5/2013 5.24 136 9/3/2013 5.69 119 10/29/2013 6.10 88.6 1/27/2014 2.16 85.7 5/19/2014 1.21 51.1 8/11/2014 1.6 67 10/21/2014 1.03 58.1 MW-30 Date Nitrate (mg/1) Date Chloride (mg/1) 6/22/2005 12.4 6/22/2005 125 9/22/2005 12.8 9/22/2005 125 12/14/2005 13.6 12/14/2005 128 3/22/2006 13.8 3/22/2006 125 6/21/2006 14.5 6/21/2006 124 9/13/2006 14.1 9/13/2006 118 10/25/2006 14.6 10/25/2006 124 3/15/2007 14.4 3/15/2007 125 8/22/2007 14.6 8/22/2007 126 10/24/2007 14.9 10/24/2007 122 3/19/2008 14.8 3/19/2008 118 6/3/2008 18.7 6/3/2008 125 8/4/2008 17.3 8/4/2008 121 11/5/2008 15.6 11/5/2008 162 2/3/2009 15.3 2/3/2009 113 5/13/2009 15.1 5/13/2009 122 8/24/2009 20.9 8/24/2009 118 10/14/2009 15.0 10/14/2009 129 1/20/2010 15.4 1/20/2010 106 2/9/2010 16.1 2/9/2010 127 4/27/2010 15.8 4/27/2010 97 5/24/2010 17.0 9/14/2010 111 6/15/2010 15.3 11/9/2010 126 8/24/2010 16.0 2/1/2011 134 9/14/2010 15.0 4/11/2011 134 10/19/2010 15.0 5/10/2011 128 11/9/2010 15.0 6/20/2011 127 12/14/2010 16.0 7/5/2011 127 1/10/2011 15.0 8/3/2011 126 2/1/2011 16.0 9/7/2011 145 3/14/2011 17.0 10/4/2011 129 4/11/2011 16.0 11/8/2011 122 5/10/2011 16.0 12/12/2011 124 6/20/2011 17.0 1/24/2012 124 7/5/2011 17.0 2/14/2012 126 8/3/2011 14.0 3/14/2012 128 9/7/2011 16.0 4/10/2012 128 10/4/2011 16.0 5/2/2012 124 11/8/2011 16.0 6/18/2012 131 12/12/2011 16.0 7/10/2012 128 1/24/2012 17.0 8/7/2012 139 2/14/2012 17.0 9/19/2012 130 3/14/2012 18.0 10/23/2012 135 4/10/2012 17.0 11/13/2012 114 5/2/2012 16.0 12/26/2012 122 MW-30 Date Nitrate (mg/1) Date Chloride (mg/1) 6/18/2012 15.0 1/23/2013 128 7/10/2012 17.0 2/26/2013 129 8/7/2012 18.0 3/20/2013 126 9/19/2012 16.0 4/17/2013 117 10/23/2012 16.2 5/15/2013 119 11/13/2012 18.5 6/25/2013 127 12/26/2012 17.2 7/10/2013 130 1/23/2013 19.2 8/20/2013 126 2/26/2013 21.4 9/18/2013 131 3/20/2013 14.3 10/22/2013 128 4/17/2013 16.8 11/20/2013 124 5/15/2013 18.8 12/18/2013 134 6/25/2013 16.1 1/8/2014 131 7/10/2013 17.6 2/25/2014 135 8/20/2013 16.4 3/11/2014 144 9/18/2013 16.9 4/23/2014 154 10/22/2013 19.7 5/14/2014 128 11/20/2013 19.5 6/3/2014 128 12/18/2013 20.7 7/29/2014 140 1/8/2014 20.3 8/20/2014 139 2/25/2014 18.4 9/9/2014 136 3/11/2014 21.3 10/7/2014 136 4/23/2014 18.3 11/10/2014 154 5/14/2014 17.9 12/10/2014 138 6/3/2014 19.4 7/29/2014 15.6 8/20/2014 13.8 9/9/2014 16.8 10/7/2014 11.0 11/10/2014 16.2 12/10/2014 17.1 Under the groundwater sampling program, accelerated monitoring for nitrate began in MW- 30 prior to when the accelerated monitoring for chloride began. This difference accounts for the different number of data points represented above. MW-31 Date Nitrate (mg/1) Date Chloride (mg/1) 6/22/2005 24.2 6/22/2005 139 9/22/2005 22.4 9/22/2005 136 12/14/2005 23.8 12/14/2005 135 3/22/2006 24.1 3/22/2006 133 6/21/2006 25.3 6/21/2006 138 9/13/2006 24.6 9/13/2006 131 10/25/2006 25.1 10/25/2006 127 3/15/2007 23.2 3/15/2007 132 3/15/2007 22.0 3/15/2007 132 8/27/2007 23.3 8/27/2007 136 10/24/2007 24.6 10/24/2007 122 3/19/2008 25.0 3/19/2008 124 6/3/2008 29.3 6/3/2008 128 8/4/2008 28.7 8/4/2008 124 11/11/2008 29.9 11/11/2008 119 2/3/2009 23.4 2/3/2009 115 5/13/2009 22.4 5/13/2009 124 8/24/2009 15.4 8/24/2009 122 10/14/2009 22.6 10/14/2009 138 2/9/2010 21.7 2/9/2010 128 4/20/2010 22.5 4/20/2010 128 5/21/2010 23.0 9/13/2010 139 6/15/2010 21.1 11/9/2010 138 8/24/2010 22.0 2/1/2011 145 9/13/2010 21.0 4/1/2011 143 10/19/2010 20.0 5/10/2011 143 11/9/2010 20.0 6/20/2011 145 12/14/2010 20.0 7/5/2011 148 1/10/2011 19.0 8/2/2011 148 2/1/2011 21.0 9/6/2011 148 3/14/2011 22.0 10/3/2011 145 4/1/2011 21.0 11/8/2011 145 5/10/2011 20.0 12/12/2011 148 6/20/2011 22.0 1/24/2012 155 7/5/2011 22.0 2/13/2012 150 8/2/2011 20.0 3/13/2012 152 9/6/2011 21.0 4/9/2012 160 10/3/2011 21.0 5/2/2012 151 11/8/2011 21.0 6/18/2012 138 12/12/2011 21.0 7/9/2012 161 1/24/2012 21.0 8/6/2012 175 2/13/2012 21.0 9/18/2012 172 3/13/2012 22.0 10/22/2012 157 4/9/2012 21.0 11/6/2012 189 5/2/2012 20.0 12/18/2012 170 MW-31 Date Nitrate (mg/1) Date Chloride (mg/1) 6/18/2012 21.6 1/22/2013 176 7/9/2012 21.0 2/19/2013 174 8/6/2012 21.0 3/19/2013 168 9/18/2012 21.0 4/16/2013 171 10/22/2012 18.0 5/13/2013 169 11/6/2012 23.6 6/24/2013 179 12/18/2012 22.2 7/9/2013 182 1/22/2013 22.8 8/19/2013 183 2/19/2013 19.3 9/17/2013 193 3/19/2013 19.1 10/23/2013 188 4/16/2013 18.8 11/18/2013 174 5/13/2013 23.8 12/17/2013 203 6/24/2013 20.0 1/7/2014 194 7/9/2013 21.7 2/17/2014 197 8/19/2013 16.0 3/10/2014 230 9/17/2013 21.2 4/28/2014 230 10/23/2013 21.2 5/13/2014 200 11/18/2013 23.9 6/2/2014 173 12/17/2013 24.2 7/28/2014 200 1/7/2014 24.0 8/18/2014 210 2/17/2014 20.6 9/3/2014 210 3/10/2014 26.2 10/6/2014 205 4/28/2014 19.1 11/4/2014 204 5/13/2014 23.3 12/9/2014 215 6/2/2014 23.1 7/28/2014 19.0 8/18/2014 15.2 9/3/2014 18.9 10/6/2014 15.9 11/4/2014 20.9 12/9/2014 17.0 Under the groundwater sampling progran, accelerated monitoring for nitrate began in MW-31 prior to when the accelerated monitoring for chloride began. This difference accounts for the different number of data points represented above. TabK Concentration Trend Graphs en c 0 .. ctl ... -c Cl) () c 0 (.) ~ ... . ~ z ,.... ... Cl) G) E 0 N Cl) c.. 0 ~ K ~ " • ~ ~ r ' O'l co 9 ~ -liBV'J ~ ~ ~ 8 ~ -6nv [> t> t j -0~-AON ' eo-1nr ~ eo-qa.::t C\1 .,..... 0 (lt6w) Ill c: 0 ".t:i ca "--c: Cl) CJ c: 0 0 Cl) "'0 "i: 0 .c: 0 T""" "-CI) a; E 0 N -~ Q. 0 0) ~ .... ---- 0 co l' ~ ~ J r---.. ( ~ ~ ..... r--..._.. 0 <D 0 0 I!) .q- (1J6W) 0 C\J 0 T""" - - 8 ~ -onv - 0 ~-/\ON so-qa.::f 0 en s:::: 0 ~ :I.. -s:::: Cl) u s:::: 0 0 .! ca :I.. .~ z N :I.. ; E 0 N Cl) c: 0'> 0 ·<.. 00 0 ~ ~ ,._ c.o 0 """""~ 0 1.() 0 (1J6W) ~ _.----r""""" ...... ~ ~ ~ ~~ ~"' ~ ~~ ~ ~ ~ >~ C\J ci ..- 0 8 ~ -6nv -O~-AON -60-1nr so-qa.:J 0 tn s:::: 0 ·~ as lo-... s:::: Q) (.) s:::: 0 (.) Q) "'C "i: 0 s:. (.) N lo-CI) Q) E 0 N .! 0.. ..... co T""" 9 ~ -ABV\1 ~ ~, ~, ., 8 ~ -Bnv .(' ~ - ~ ~ ~v· 0~-AON ~~ ~ _,.. eo-qa.:1 C\1 0 co 0 T""" (1/fiW) f/) c 0 +:: cu lo-... c G) (.) c 0 (.) G) ... cu lo-::: z M lo- G) ... G) E 0 N G) c:: C\J (1t6w) 1.0 c::) 0 t~-oaa 8~-Bnv G ~-JdV 0~-AON 1/) c 0 "+=i ~ """ -c Cl) (.) c 0 (.) Cl) "C "i: 0 .c (.) M """ i E 0 N Cl) ii: 0 '<t ..- 0 (\J ..- .... 0 0 ..- 0 <Xl (1/BW) ~ ~ ' ~ < ~ ~ ~ .. ~ 0 (0 ~ 0 '<t ... «:: "' ~ 0 (\J g ~ -AeV\l - 8 ~ -Bnv - -0 ~-/\ON 6o-1nr so-qa:J 0 tn c: 0 ... m .... -c: Cl) (.) c: 0 (.) Cl) 1a .... . ~ z \ ~ ~ 4 ..... ~ ~ " > ,..-co 0 (1J6W) ~ ~ \ ~ ~ ~ "' ~~ ~ /~ (() 0 C\J 0 - - 0 9 ~ -AEV\1 v~-oaa 8 ~ -Bnv 0~-AON eo-1nr ao-qa.:J In c: 0 -.::; as ... -c: G> () c: 0 (.) G> "tJ 'i: .2 J: (.) """ I z ~ j-------.-------r------,-------.-----~~----~------,·9~-Ae~ v~-oaa -8 ~-onv -c ~-JdV 0~-AON 1------+-------+--------t-------;------t-------+-------+ so-qa.:J 0 C') LO C\J 0 C\J (1t6w) 0 LO 0 ,..- (/) c 0 "+::0 ~ :r.. -c Cl) (.) c 0 (.) Cl) -~ :r.. ~ z N I z 3: 1- r-------~-------,--------~-------.--------.--------.9~-Ae~ 17~-oaa 8~-5nv ~ c~-JdV 0 ~-/\ON 6o-1nr ~------~-------4--------+--------+--------~-------+Bo-qa~ 0 C\J 0 0 0 00 0 (.0 (1/6W) 0 C\J 0 tn c: 0 -.:::; m ... -c: C1) () c: 0 (.) C1) 't' 'i: .2 .c: (.) N I z 3: 1- ,.-----.-------r----...-----,-----r----...,-g ~-ABV\1 17~-oao 8 ~ -5ny c ~ -Jd'v' ~0~·/\0N 60·1nr ~----r----~----~----+----~-----r eo-qa~ 0 N ,.- 0 0 ,.- 0 ex:> 0 <D 0 N 0 (/) c 0 '.t:i m ... -c Q) (.) c 0 (.) Q) -m ... . t:: z M I z 3: t- ~----~-------r------.-------~----~~-----.-------r 9~-Ae~ · v ~-oaa 8 ~ -6nv -l ~ -Jd'tf 0~-AON ~----~-------+------,_------+-----~r------+-------+80-qa~ 0 ('I) 1.{) C\J 0 C\J (1f6W) 1.{) 0 1.{) 0 1/) c 0 ".+:0 t1S ... -c Cl) (J c 0 0 Cl) "'C "i: 0 ~ 0 M I z ~ 0 0 C\J 0 co .- \ ~ ~ < 0 CD 0 C\J ~ 0 0 ~ (1f6W) 0 co 0 CD 0 ~ 0 C\J . - 0 9~-li'BII\I 17~-oao 8 ~ -Bnv 0 ~-/\ON 60-lnr eo-qa.::1 en s::::: 0 ; C'a :1.. -s::::: Cl) u s::::: 0 () Cl) -C'a :1.. ~ z "'=t I z s: I- ~--------~--------~--------~----------.----------r 9kAB~ -s ~ -5nv c:a -JdV 0 ~-/\ON 6o-1nr ~--------+---------4---------~---------r---------+so-qa~ C\1 l{) c:i 0 (/) c 0 '+=i m ... -c Q) u c 0 (.) Q) , "i: .2 .c (.) o::t I z s: ~ .----.-----.------,,....---.----.----r---.,-----,-9 ~ -ABII'J -8 ~ -5ny c ~ -Jd'v' 0 ~-liON 6o-1nr ~----,_---+--~~--~---r----;---+----+90-qa~ 1.{) C') 0 C') 1.{) C\J 0 C\J (1/BW) 1.{) 0 0 ,.-,.- If) t: 0 ·.;:::; ca II.. -t: Q) (.) t: 0 0 Q) -ca II.. ~ z ,.... I z 3: 1- .------.-------.-------,.------~-----.-s ~ -1nr v~-unr 8~-AON 8 ~-keV\1 "Z~-PO z ~ -Jd'v' ~ ~-das ~ ~ -qa.:l o ~ -Bnv o~-uer 1-------+------1------+------"'-------1-6o-1nr C\1 (1/BW) l.{) c) 0 ~------~------~--------~------~--------~-------r 9~-Ae~ 8 ~-Bnv 1/) c 0 ·.;::; cu ... -c Cl) (,) c c~-JdV 0 (.) Cl) "C "i: 0 .c (.) ....... I z 3: ... O~·AON -60·1nr 1--------t---------l---------+--------+----------,l---------+ Bo-qa~ C\J 0 C\J 0 ..- .-------.---------.------.-----.,--------,-s ~ -1nr -17~-oao 17~-unr 8~-AON . £ ~ -ABV'J en s:::: 0 ; cu :1.. -G ~-lOO s:::: Cl) (.) s:::: 0 (.) Cl) c~-JdV -cu :1.. := z co ""'" I z ~ ~-das 3: 1- ~ ~-qa.:l o~-Bnv o~-uer 1-------t------t-------11------+-------+ so-1nr I!) C\1 I!) 0 C\i 0 (1J6W) tn c 0 ~ m ... -c G) u c 0 (..) G) "C 'i: 0 J: (..) co T"' I z 3: 1- r----.----,r-----.--......... ---.-------.------.----.----.-s ~ -1nr -17~-unr -8 ~-/\ON -8 ~ -AeV\1 -<::~-PO Z: ~ -Jd'v' ~ ~-das -~ ~-qa.:J -o ~-Bnv -0~-uer 1----+---1---11-------l-----t---I-----+---+---J.-eo-1nr 0 0> 0 00 0 (!) 0 0 l{) """ (1/BW) 0 C\J 0 T- 0 9 0 0 7/1/2002 11/1/2002 3/1/2003 7/1/2003 11/1/2003 3/1/2004 7/1/2004 11/1/2004 - 3/1/2005 7/1/2005 11/1/2005 3/1/2006 7/1/2006 11/1/2006 3/1/2007 7/1/2007 11/1/2007 3/1/2008 7/1/2008 11/1/2008 - 3/1/2009 7/1/2009 11/1/2009 3/1/2010 7/1/2010 11/1/2010 3/1/2011 7/1/2011 11/1/2011 3/1/2012 - 7/1/2012 ~ 11/1/2012 . 3/1/2013 - 7/1/2013 11/1/2013 3/1/2014 7/1/2014 1-" 0 0 0 N 0 0 0 w 0 0 0 .j:>, 0 0 0 V1 0 0 0 en 0 0 0 -....! 0 0 0 --4 :E ~ I ~ U) z -· r+ """ Q,) r+ tl) n 0 ::l n tl) ::l r+ """ Q,) r+ -· 0 ::l "' 0 12/1/2005 3/1/2006 . 6/1/2006 - 9/1/2006 12/1/2006 3/1/2007 6/1/2007 •. 9/1/2007 12/1/2007 3/1/2008 6/1/2008 9/1/2008 12/1/2008 3/1/2009 6/1/2009 9/1/2009 12/1/2009 3/1/2010 6/1/2010 - 9/1/2010 •. 12/1/2010 3/1/2011 - 6/1/2011 - 9/1/2011 12/1/2011 - 3/1/2012 6/1/2012 9/1/2012 12/1/2012 -· 3/1/2013 6/1/2013 9/1/2013 12/1/2013 3/1/2014 6/1/2014 - 9/1/2014 -1 lJ1 0 ....... 0 0 ....... lJ1 0 N 0 0 N lJ1 0 -1 ~ ,J::. I ...... \0 n ::r -0 ""'': -· a. tl) n 0 :::::J n tl) :::::J r+ ""'': QJ r+ -· 0 :::::J V) 0 0 5/1/2005 8/1/2005 - 11/1/2005 2/1/2006 5/1/2006 8/1/2006 11/1/2006 2/1/2007 -1 5/1/2007 .I 8/1/2007 11/1/2007 2/1/2008 5/1/2008 8/1/2008 11/1/2008 2/1/2009 5/1/2009 8/1/2009 - 11/1/2009 2/1/2010 5/1/2010 8/1/2010 - 11/1/2010 2/1/2011 5/1/2011 8/1/2011 11/1/2011 2/1/2012 5/1/2012 8/1/2012 11/1/2012 2/1/2013 - 5/1/2013 - 8/1/2013 - 11/1/2013 2/1/2014 5/1/2014 - 8/1/2014 - N 0 ~ 0 C'l 0 90 0 f-\ 0 0 f-\ N 0 f-\ ~ 0 f-\ C'l 0 -1 ~ ~ I N ...... z -· ,... .., QJ ,... tt) n 0 ::::s n tt) ::::s ,... .., QJ ,... -· 0 ::::s "' 0 12/1/2005 3/1/2006 6/1/2006 9/1/2006 12/1/2006 3/1/2007 6/1/2007 9/1/2007 12/1/2007 3/1/2008 6/1/2008 9/1/2008 12/1/2008 - 3/1/2009 6/1/2009 9/1/2009 12/1/2009 3/1/2010 6/1/2010 9/1/2010 - 12/1/2010 3/1/2011 6/1/2011 . 9/1/2011 12/1/2011 3/1/2012 6/1/2012 9/1/2012 12/1/2012 3/1/2013 6/1/2013 9/1/2013 - 12/1/2013 3/1/2014 6/1/2014 '" 9/1/2014 U'1 0 ..... 0 0 ..... U'1 0 N 0 0 N U'1 0 w 0 0 w U'1 0 .p. 0 0 -1 ~ ~ I N ~ n :::r -0 ~ -· c. t'D n 0 ::s n t'D ::s ,.... ~ QJ ,.... -· 0 ::s "' 2/28/2007 6/27/2007 8/15/2007 10/10/2007 3/26/2008 6/25/2008 9/10/2008 10/15/2008 3/11/2009 6/24/2009 9/15/2009 12/29/2009 3/3/2010 6/15/2010 8/12/2010 8/24/2010 10/13/2010 2/23/2011 6/1/2011 8/17/2011 11/16/2011 1/19/2012 6/13/2012 9/12/2012 10/4/2012 2/11/2013 6/5/2013 9/3/2013 10/29/2013 1/27/2014 5/19/2014 8/11/2014 10/21/2014 0 r ..... 0 N 0 w 0 mg/L ~ 0 U'l 0 0"1 0 -...! 0 -1 ~ ~ I N N z -· r+ """' ~ r+ tD n 0 ::s n tD ::s r+ """' ~ r+ -· 0 ::s "' 2/28/2007 6/27/2007 8/15/2007 10/10/2007 3/26/2008 6/25/2008 9/10/2008 10/15/2008 3/11/2009 6/24/2009 9/15/2009 12/29/2009 3/3/2010 6/15/2010 8/12/2010 8/24/2010 10/13/2010 2/23/2011 6/1/2011 8/17/2011 11/16/2011 1/19/2012 6/13/2012 9/12/2012 10/4/2012 2/11/2013 6/5/2013 9/3/2013 10/29/2013 1/27/2014 5/19/2014 8/11/2014 10/21/2014 1-> 0 0 0 N 0 0 (JJ 0 0 mg/L ~ 0 \.11 0 0 en 0 0 '-1 0 0 -I :E ~ I N N n ::::r -0 """' -· a. tD n 0 ::::s n tD ::::s ~ Ql ~ -· 0 ::::s U) z lll:t N I lll:t s 1- V) c 0 ·-+"' tU ... +"' c cu u c 0 u cu "'C ·-... 0 ..c: u ~ N I ~ ~ 0 0 '<:t .--1 0 0 N .--1 0 0 0 .--1 0 0 00 l/8W 0 0 \.0 0 0 '<:t 0 0 N 0 U) s::::: 0 ·-+"' ns L. +"' s::::: Q) u s::::: 0 u Q) +"' ns L. +"' ·-z Ln N I "" ~ l/8W "' c: 0 ·-+"' tU '-+"' c: <U u c: 0 u <U "'C ·-'-0 .s:. u Ln N I .q- ~ ..... 0 0 o::t 0 Ll'l M 0 0 M 0 Ll'l N 1/SW 0 0 N 0 L{') .-4 0 0 .-4 0 L{') 0 ..... ..... N N 0 ll1 0 ~ 0 ll1 0 0 0 0 0 0 6/1/2005 . 9/1/2005 12/1/2005 3/1/2006 6/1/2006 9/1/2006 - 12/1/2006 3/1/2007 6/1/2007 9/1/2007 12/1/2007 3/1/2008 6/1/2008 s 9/1/2008 -~ 12/1/2008 I w 3/1/2009 0 6/1/2009 z -· ,... 9/1/2009 ""' QJ ,... 12/1/2009 tD 3/1/2010 n 0 6/1/2010 -::l n 9/1/2010 tD ::l 12/1/2010 ,... ""' QJ 3/1/2011 ,... -· 6/1/2011 0 ::l 9/1/2011 "' 12/1/2011 - 3/1/2012 - 6/1/2012 - 9/1/2012 12/1/2012 . 3/1/2013 6/1/2013 9/1/2013 12/1/2013 - 3/1/2014 6/1/2014 9/1/2014 .. 12/1/2014 6/1/2005 9/1/2005 0 12/1/2005 3/1/2006 •. 6/1/2006 9/1/2006 . 12/1/2006 - 3/1/2007 . 6/1/2007 9/1/2007 12/1/2007 3/1/2008 - 6/1/2008 9/1/2008 12/1/2008 3/1/2009 6/1/2009 9/1/2009 12/1/2009 3/1/2010 6/1/2010 9/1/2010 12/1/2010 3/1/2011 6/1/2011 . 9/1/2011 - 12/1/2011 3/1/2012 ' 6/1/2012 - 9/1/2012 12/1/2012 3/1/2013 6/1/2013 9/1/2013 12/1/2013 3/1/2014 6/1/2014 9/1/2014 12/1/2014 N 0 """' 0 CTI 0 00 0 ....... 0 0 ....... N 0 ....... """' 0 ....... CTI 0 ....... 00 0 s ~ I w 0 n ~ -0 ""'' -· c. CD n 0 :J n CD :J ~ Ql ~ -· 0 :J "' 0 0 6/1/2005 - 9/1/2005 12/1/2005 3/1/2006 6/1/2006 9/1/2006 12/1/2006 3/1/2007 6/1/2007 9/1/2007 12/1/2007 3/1/2008 6/1/2008 . 9/1/2008 12/1/2008 - 3/1/2009 6/1/2009 9/1/2009 12/1/2009 3/1/2010 6/1/2010 . 9/1/2010 ~· 12/1/2010 3/1/2011 6/1/2011 - 9/1/2011 . 12/1/2011 3/1/2012 - 6/1/2012 - 9/1/2012 12/1/2012 3/1/2013 . 6/1/2013 9/1/2013 12/1/2013 3/1/2014 6/1/2014 9/1/2014 12/1/2014 l..n 0 1-' 9 0 1-' l..n 0 N 9 0 N l..n 0 w 0 0 w l..n 0 s :E I w ~ z -· r+ @ r+ t1) n 0 ::::s n t1) ::::s r+ @ r+ -· 0 ::::s "' 0 6/1/2005 9/1/2005 12/1/2005 3/1/2006 6/1/2006 9/1/2006 12/1/2006 3/1/2007 6/1/2007 9/1/2007 . 12/1/2007 3/1/2008 " 6/1/2008 . 9/1/2008 - 12/1/2008 3/1/2009 . 6/1/2009 . 9/1/2009 12/1/2009 3/1/2010 - 6/1/2010 9/1/2010 12/1/2010 3/1/2011 6/1/2011 9/1/2011 12/1/2011 3/1/2012 6/1/2012 9/1/2012 12/1/2012 3/1/2013 6/1/2013 9/1/2013 .. 12/1/2013 - 3/1/2014 - 6/1/2014 9/1/2014 12/1/2014 U1 0 ...... 0 0 ...... U1 0 N 0 0 N U1 0 s: :E I w ~ n :::r -0 ~ -· c. n> n 0 ::::s n n> ::::s ,... ~ QJ ,... -· 0 ::::s "' TabL CSV Transmittal Letter Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Lundberg, Kathy Weinel Monday, February 23,2015 10:15 AM Rusty Lundberg 'Phil Goble'; 'Dean Henderson'; Harold Roberts; David Frydenlund; Scott Bakken; David Turk; Jaime Massey; Dan Hillsten Transmittal of CSV Files White Mesa Mill 2014 04 Nitrate Monitoring 04 2014 Nitrate EDD.csv Attached to this e-mail is an electronic copy of laboratory results for nitrate monitoring conducted at the White Mesa Mill during the fourth quarter of 2014, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel 1 Tab M Residual Mass Estimate Analysis Figures and Tables Tah M -Figures 50000 -~----------------------------------------------------------------~ 45000 -1 ------ 40000 .............. :0 35000 :::::::. ~ ------~--- U) U) e 3oooo z I 0 z 25000 -1---------- Q) E :::J Q. 20000 , ! E 15000 ; U) w 10000 5000 -~l I . 0 .....,_plume mass estimate (lb) J .:::::_-Linear (plume mass estimate (lb)) baseline 01 2013 02 2013 03 2013 H:\718000\feb15\nitrate\TimeSeries.xls: mass (F M.1 )a -~--- 04 2013 01 2014 HYDRO GEO CHEM,INC. 02 2014 Approved !';.I!'; 03 2014 04 2014 ESTIMATED RESIDUAL MASS OF NITRATE (AS N03-N) PLUME Figure M_1 g 50000 .-------~~--- 111 Ill ca E Cll 40000 E :J ii '0 .! 30000 +-------------ca E -~ --+--Plume mass estimate (lb) w 20000 -- 120 - 100 ,.----~-~ 80 60 20 I ,--__....,_ "N03-N c:;:-ntration -(m-g-/L-)-~ 0 90 ------------------------------------- g Ill Ill Cll c: ~ u :E - 75 ~ 60 45 -y-------------------------------- 30 15 j__ 0 , _ -Sat~hickness _(It_) __ j ----------------1 0.08 ..,....---------------------------------, 0.06 0.04 0.02 +---------------~----- 0 1 [ ~lbs N03-N/ttQ--.------..- HYDRO GEO CHEM, INC. TIME SERIES FOR N03-N PLUME MASS ESTIMATES AND TWN-2 [N03-N], SATURATED THICKNESS, AND lbs N03-N/te XX H:\718000\feb15\nitrate\TimeSeries.xls: TWN-2P (F M.2) i 50000 1 E .. .. ~ 4oooo I ! I .l!l 30000 I'll E ;: ~ -+-Plume mass estimate (lb) g (I) (I) Cll c: .::tt:. .!::! .c - "' = z 20000 ------ 120 ---~- 100 80 60 __.,._ N03-N concentration (mg/L_l _] --=====----~---- 40 --- 20 0 80 ~1---------------------------------------1 64 --~,.---~-.----•r----•----~·----~-.---~ • ._ ____ _ 48 ---·--------- 32 ·r-- 16 l_____======~~~~--------------------, _ • Saturated thickness (It) J 0 ---- 0.08 .,----------------------------, --+-lbs N03-Nffl2l 0.06 (s 0.04 z (I) :!:! 0.02 ~~·~--~~~--~ • .---~·._--~·.----. I 0 -t-----------...--• - HYDRO GEO CHEM, INC. TIME SERIES FOR N03-N PLUME MASS ESTIMATES AND TWN-3 [N03-N], SATURATED THICKNESS, AND lbs N03-Ntte H:\718000\feb15\nitrate\TimeSeries.xls: TWN-3P (F M.3) ~ 50000 .----------------------------- "' "' Ill ~ 40000 I E ~ j 30000 J Ill E ~ j--+--Plume mass estimate (I b) "' = ~ "' 0 z "' ::5! 20000 ------ 120 100 "t - __ __...,_ N03-N concentration (mg/L~ ao I so r------------~ ------------------------------------- 4o l -----_j 20 0 • .---~·----~·~--~ • ._---.~--~·~--~·.__---* ~ 1 90 ~-----------------------------------· :: t--.----.---.----------------------~=~----1 45 • ---. ... t---·f---------------• • 30 t-------------------------------------------------~ 15 l -Saturated thickness (It) J 0 ~======~====~~----------------- 0.08 ~ lbs N03-N/ft2 006 j 0.04 0.02 • • • • • • .. • -• 0 ,...--..--- HYDRO GEO CHEM, INC. TIME SERIES FOR N03-N PLUME MASS ESTIMATES AND TW4-21 [N03-N], SATURATED THICKNESS, AND lbs N03-Ntte XX M.4 H:\718000\feb15\nitrate\TimeSeries.xls: TW4-21 P (F M.4) g: 50000 Ill Ill I'll E 111 40000 E ::J Q. "0 .l!! 30000 I'll E ~ I ~Plume mass estimate (lb) 20000 ..J..---- 120 -~---j 100 • N03-N concentration (mg~ 80 ------ g Ill Ill 111 I: .:.e. (J :c - 60 40 20 0 ---- 90 45 +------------------ 30 ~------------------------------------------------~ 15 ~==========~- -Saturated thickness (ttc=J 0 0.08 ,..---------------------~---------~ "'= z 0.06 d' 0.04 z Ill :e 0.02 0 L ___._lbs N03-N/ft2 I !- r: -.- 0 .._<:> .._<:> ~~ ~\) ~\) r:;,0 'O'b' cY 0~ .._<:> ~\) & H:\718000\feb15\nitrate\TimeSeries.xls: TW4-22P (F M.5) .._<:> ~\) d' ~ .._b< ~\) ~\) cY 0~ HYDRO GEO CHEM, INC. .._b< .._b< ~\) ~\) & d' TIME SERIES FOR N03-N PLUME MASS ESTIMATES AND TW4·22 [N03·N], SATURATED THICKNESS, AND lbs N03-Ntte ,._ .... XX g: 50000 ----~ Ill Ill 111 E Cll 40000 E :I i 30000 1 ~ I Plume mass estimate ~~ 20000 -------- 120 ..------ 100 +:--=====-----==--~=---..:.; I _ ____...._ N03-N concentration (mg/L) J 80 --==----- 60 40 r --=-- 20 _J_:_ __ 0 90 r--------::r_ - -1 ; 1-----. _ ____.______ 45 -----tlt:----:11:·==~~=-----l 30 "if-=.-s .. ,rn"' "'"'oo~-=~=n)==--~ 0 0.08 ---------------- __J I I ' • lbs N03-N/It2 0.06 .• -------------------- 0.04 j 0.02 --=•<=---...... ~.. -_.A o4·t---ee-..;::;::::::=-:==:==:•=====-:==:::• ...--.............--. --· -. . 0 -1-----,.-----,,------.------.----.---.,.- H:\718000\feb15\nitrate\TimeSeries.xls: TW4-24P (F M.6) HYDRO GEO CHEM, INC. TIME SERIES FOR N03-N PLUME MASS ESTIMATES AND TW4-24 [N03-N], SATURATED THICKNESS, AND lbs N03-N/te XX g 50000 Ul Ul ca E Q) 40000 E ::I c. , ~ 30000 -----~--------------------­ca E ~ w ::J c, §_ z \.., 0 ~ g Ul Ul Q) c ..lll: (J :E -, Q) -~ ::I 'lii en 20000 120 100 --+--Plumen;ass estimate (I b) J 80 _...,__ N03-N concentration (mg/Wj ----- :: l 20 0 90 ~ -----~-=~v 75 • 60 45 ....------------ 30 t-=; 15 --------- .-----Saturated thickness (It) J o-- -- __ j o.oa T-----------------------------------------------~ ........__ lbs N03-N/ft2 o.a.L "' ;:: z ..., 0.04 0 z Ul ::e 0.02 \ 0 ~. jl H:\718000\feb15\nitrate\TimeSeries.xls: TW4-25P (F M.7) • • HYDRO GEO CHEM, INC. TIME SERIES FOR N03-N PLUME MASS ESTIMATES AND TW4-25 [N03-N], SATURATED THICKNESS, AND lbs N03-N/te XX g: 50000 Ill ~40000 p f 30000 I ____________ _ ell I E ·;; ~Plume mass estimate {lb) w 20000 120 ------ 100 J ::J l __...,_ N03-N concentration (mg/L) -c, 80 .§. 60 z I .., 0 40 ~ 20 -..=-• * • • 0 90 -, 75 t------C • Saturated thickness {ft) J 60 45 ·1---------------------------f 30 --··~---~·-=--••t===ll•l===ll•l==--l•l--~""'=iii•I---=--=--=-=II•I--"""'--=--=-•1-...J 1 :-+---1 ----··1 0.08 ~ c .......,_lbs N03-N/ft2 0.06 ---- z d' 0.04 r---------------------------1 z Ill :e 0.02 +---------------------------1 • • • • • 0 H:\71BOOO\feb15\nitrate\TimeSeries.xls: MW-30P (F M.B) • HYDRO GEO CHEM, INC. • • • TIME SERIES FOR N03-N PLUME MASS ESTIMATES AND MW-30 [N03-N], SATURATED THICKNESS, AND lbs N03-N/te XX :c 50000 I 40000 ~ a. "D ,S! 30000 Ill ~ l ~Plume mass estim~e (I b) 20000 ---- 120 100 ___..,_ N03-N concentration (mg/L) 80 60 ::c: 0 90 g 75 .:...._ ________________ ------------1 Cll Cll I» c ~ u :c - "' ;:: ~ "' 0 z Cll a 60 ~·-.--=~~-.--~-~----·~--~----~-.--~·~==~-··~==~·· 45 30 "------ 15 -----~------------~ :I -Saturated thick~tll 0 0.08 l 0.06 0.04 0.02 0 HYDRO GEO CHEM, INC. -:j TIME SERIES FOR N03-N PLUME MASS ESTIMATES AND MW-31 [N03-N], SATURATED THICKNESS, AND lbs N03-N/ft2 .... XX M.9 H:\718000\feb15\nitrate\TimeSeries.xls: MW-31 P (F M.9) Tab M -Tables Rank 1 2 3 4 5 6 7 8 Method Table M.1 Well Rankings Based on Methods 1-1 0 Method 1 Method 2 Method 3 TWN-2 TW4-25 TWN-2 TW4-22 TWN-2 TW4-22 TW4-24 MW-31 TW4-24 TWN-3 TW4-21 MW-31 MW-31 TWN-3 TWN-3 MW-30 TW4-22 TW4-21 TW4-21 TW4-24 MW-30 TW4-25 MW-30 TW4-25 1 Average [N03-N] 2 Average well saturated thickness 3 Average lbs N03-N/ft2 Method 4 Method 5 Method 6 TWN-2 TW4-24 TW4-24 MW-31 TWN-2 TWN-2 MW-30 MW-31 MW-31 TW4-22 TW4-22 TW4-22 TWN-3 MW-30 MW-30 TW4-25 TW4-25 TW4-25 TW4-21 TWN-3 TWN-3 TW4-24 TW4-21 TW4-21 4 Remove well from mass estimate (plume boundary not fixed) 5 Increase [N03-N] by 20% (plume boundary not fixed) 6 Decrease [N03-N] by 20% (plume boundary not fixed) 7 Decrease saturated thickness by 20% (plume boundary not fixed) Method 7 TW4-24 TWN-2 MW-31 TW4-22 TW4-25 TWN-3 MW-30 TW4-21 8 Mass N03-N per well based on polygonal estimator (plume boundary fixed). 9 Volume per well based on polygonal estimator (plume boundary fixed). 10 Average [N03-N] per well based on polygonal estimator (plume boundary fixed). H:\718000\feb15\nitrate\Rankings.xls Method 8 Method 9 Method 10 TW4-24 TW4-24 TWN-2 TWN-2 TWN-2 TW4-22 TW4-22 MW-31 TW4-24 MW-31 TW4-22 MW-31 MW-30 MW-30 TWN-3 TWN-3 TWN-3 TW4-25 TW4-25 TW4-25 TW4-21 TW4-21 TW4-21 MW-30 TableM.2 Scoring of Results: Methods 1 through 3 weiiiD score combined rank TWN-2 4 1 TW4-22 10 2 MW-31 12 3 TW4-24 13 4 TWN-3 14 5 TW4-21, TW4-25 17 6 MW-30 21 7 Table M.3 Scoring of Results: Methods 4 through 7 weiiiD score combined rank TWN-2 7 1 TW4-24, MW-31 11 2 TW4-22 16 3 MW-30 19 4 TW4-25 23 5 TWN-3 25 6 TW4-21 31 7 Table M.4 Scoring of Results: Methods 8 through 10 weiiiD score combined rank TWN-2 4 1 TW4-22 10 2 MW-31 12 3 TW4-24 13 4 TWN-3 14 5 TW4-21, TW4-25 17 6 MW-30 21 7 Table M.5 Scoring of Results: Methods 3 and 8 weiiiD score combined rank TWN-2 3 1 TW4-24 4 2 TW4-22 5 3 MW-31 8 4 TWN-3 11 5 MW-30 12 6 TW4-21 14 7 TW4-25 15 8 Note: scores are sums of ranks from Table M.1 H:\718000\feb15\nitrate\Rankings.xls Table M.6 Scoring of Results: Methods 1 through 10 weiiiD score combined rank TWN-2 16 1 TW4-24 29 2 MW-31 34 3 TW4-22 35 4 TWN-3 56 5 MW-30 58 6 TW4-25 60 7 TW4-21 71 8 Note: scores are sums of ranks from Table M.1 H:\718000\feb15\nitrate\Rankings.xls