DRC-2014-007026 - 0901a068804c0b7a

'ENERGYFUELS
Energy Fuels Resources (USA) Inc.
225 Union Blvd. Suite 600
Lakewood, CO, US, 80228
303 974 2140
www.energyfuels.com DRC-2014-007026
November 24, 2014
Sent VIA OVERNIGHT DELIVERY
Mr. Rusty Lundberg
Director
Division of Radiation Control
Utah Department of Environmental Quality
195 North 1950 West
P.O. Box 144850
Salt Lake City, UT 84114-4820
Re: Transmittal of Annual Tailings Wastewater Monitoring Report
Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill
Dear Mr. Lundberg:
Enclosed are two copies of the White Mesa Uranium Mill Annual Tailings Wastewater Monitoring
Report for 2014 as required by the Groundwater Quality Discharge Permit UGW370004, as well as
two CDs each containing a word searchable electronic copy of the report.
If you should have any questions regarding this report please contact me.
Yours very truly,
Jaime Massey
Regulatory Compliance Specialist
cc: Scott A. Bakken
Harold R. Roberts
David E. Turk
Kathy Weinel
Dan Hillsten
White Mesa Uranium Mill
2014 Annual Tailings Cells Wastewater Sampling
Report
State of Utah
Groundwater Discharge Permit No. UGW370004
~·~ rr;~ERGYFUELS
Prepared by:
Energy Fuels Resources (USA) Inc.
225 Union Boulevard, Suite 600
Lakewood, CO 80228
November 24,2014
TABLE OF CONTENTS
1.0 INTRODUCTION ..................................................................................................................... 1
2.0 SUMMARY OF MILL TAILINGS ACTIVITIES IN 2013 .................................................... 1
2.1 Cell1 .................................. ! .................................................................................................. 1
2.2 Cell2 ..................................................................................................................................... 2
2.3 Cell 3 ................................................................................................ ._ ................................... 2
2.4 Cell 4A .................................................................................................................................. 2
2.4 Cell4B ................................................................................................................................... 2
3.0 SAMPLING EVENTS AND SAMPLING METHODOLOGY .............................................. 2
3.1 Sampling Events ................................................................................................................... 2
3.2 Field Data .............................................................................................................................. 3
3.3 Sampling Methodology, Equipment and Decontamination Procedures ............................... 3
3.3.1 Tailings Cells ............................................................................................................ ; .... 3
3.3.2 Cel12 Slimes Drain ........................................................................................................ 3
3.3.3 Cell4A Leak Detection Systems ................................................................................... 4
3.3.4 Cell4B Leak Detection Systems .................................................................................... 4
3.3.5 Cells 1, 2, 3, ................................................................................................................... 4
3.4 Field QC Samples ............................................................................... , ................................. 4
3.5 Laboratory Results ................................................................................................................. 4
4.0 QUALITY ASSURANCE AND DATA EVALUATION ........................................................ 4
4.1 Adherence to Sampling Plan and Permit Requirements ....................................................... 5
4.2 Analyte Completeness Review ............. , ............................................................................... 5
4.3 Data Validation ...................................................................................................................... 5
4.3.1 Field Data QA/QC Evaluation ....................................................................................... 6
4.3.2 Holding Time Evaluation ............................................................................................... 6
4.3.3 Laboratory Receipt Temperature Check ........................................................................ 6
4.3.4 Analytical Method Check .............................................................................................. 6
4.3.5 Reporting Limit Evaluation ........................................................................................... 6
4.3.6 Trip Blank Evaluation .................................................................................................... 7
4.3.7 QA/QC Evaluation for Sample Duplicates .................................................................... 7
4.3.8 Radiologies Counting Error ........................................................................................... 8
4.3.9 Laboratory Matrix QC Evaluation ................................................................................. 9
4.3.10 Gross Alpha ................................................................................................................... 11
5.0HISTORICDATA .................................................................................. , ............................... 11
6.0 SUMMARY AND CONCLUSIONS ...... , .............................................................................. 11
6.1 Cell1 .................................................................................................................................... 11
6.2 Cell 3 ................................................................................................................................... 12
6.3 Cell4A ................................................................................................................................. 12
6.4 Cell4B ................................................................................................................................. 13
6.5 Cell2 Slimes Drain .................................................... ,; ....................................................... 14
6.6 Cells 3, 4A and 4B Slimes Drain ........ ; ............................................................................... 14
6.7 Cell 2 Leak Detection System ............................................................................................. 15
6.8 Cells 1 and 3 Leak Detection System ................................................................................. 15
6.9 Cell4A Leak Detection System .......................................................................................... 15
6.10 Cell4B Leak Detection System ........................................................................................ 15
6.11 Summary and Conclusions of Analytical Results ............................................................. 16
7.0 CORRECTIVE ACTION REPORT ....................................................................................... 16
7.1 Assessment of Corrective Actions from Previous Period ................................................... 16
7.0 SIGNATURE AND CERTIFICATION ...................................................... _ ........................... 17
11
LIST OF TABLES
Table 1 Summary of Tailings Cell Wastewater Monitoring
INDEX OF TABS
Tab A Tailings and Slimes Drain Field Sheets
Tab B Sample Location Figures
Tab C Laboratory Analytical Reports
Tab D Chemical and Radiological Summary Tables
Tab E Quality Assurance and Data Validation Tables
E-1 Holding Time Evaluation
E-2 Laboratory Receipt Temperature Check
E-3 Analytical Method Check
E-4 Reporting Limit Evaluation
E-5 Trip Blank Evaluation
E-6 QA/QC Evaluation for Sample Duplicates
E-7 Radiologies Counting Error
E-8 Laboratory Matrix QC Evaluation
iii
2014 ANNUAL TAILINGS CELLS WASTEWATER SAMPLING REPORT
1.0 INTRODUCTION
This is the 2014 Annual Tailings Cells Wastewater Sampling Report for the Energy Fuels
Resources (USA) Inc. ("EFRI") White Mesa Mill (the "Mill"), as required under Part I.F.9 of the
Mill's State of Utah Groundwater Discharge Permit No. UGW370004 (the "Permit") and Section
6.0 of the Mill's Sampling and Analysis Plan for Tailings Cells Leak Detection Systems and
Slimes Drains, Revision: 2.1, dated July 30, 2012 (the "Sampling Plan") and approved by the
State of Utah Division of Radiation Control (the "DRC") on August 2, 2012.
Tailings and slimes drain sampling is required under the Sampling Plan and Part I.E.l 0 of the
Permit to be conducted on an annual basis in August of each year for the solutions in tailings
Cells 1, 3, 4A, and 4B, the solutions in the slimes drains in Cells 2, 3, 4A, and 4B (for Cells 3,
4A and 4B after the commencement of dewatering), the solutions in the leak detection system
(the "LDS") in Cell4A and 4B and any detected solutions in the LDS in Cells 1, 2, and 3 at the
time of the August Sampling event. The results of the sampling event are required to be reported
to the DRC with the Mill's Third Quarter Groundwater Monitoring Report due December 1, of
each year.
2.0 SUMMARY OF MILL TAILINGS ACTIVITIES IN 2014
This section provides a brief description of each tailings impoundment at the Mill, and any
changes that were made as a result of Mill activities during the reporting year. A description of
which systems were sampled is provided in Section 3.0.
The Mill is designed not to discharge to groundwater or surface waters. Instead, the Mill utilizes
tailings and evaporation cells for disposal of Mill effluents as indicated below:
• Cell 1: dedicated to evaporation of Mill waste solutions;
• Cell 2: contains Mill tailings, has an interim cover and is closed to future tailings
disposal;
• Cell 3: contains Mill tailings and is in the final stages of filling;
• Cell4A: receives Mill tailings and is used for evaporation of Mill solutions; and
• Cell 4B: is used for evaporation of Mill solutions.
2.1 Cell1
Cell 1 is a 55-acre impoundment built in June of 1981. It operates as an evaporation pond which
receives solutions only. Cell 1 is equipped with a LDS. In 2014, Cell 1 received fluid from the
Mill process, storm water run-off, and Mill laboratory waste. The LDS in Celli was dry in 2014.
1
2.2 Cell2
Cell 2 is a 67-acre impoundment built in May of 1980. Cell 2 was taken out of service and
covered with interim cover in 2008. Cell 2 is equipped with a LDS, and a slimes drain. The LDS
was dry in 2014. As part of closure activities, EFRI began monitoring the slimes drain system in
2008. The fluid from the slimes drain is pumped to Cell 4A. Cell 2 no longer receives any
solutions or solids.
2.3 Cell3
Cell 3 is a 71-acre impoundment built in September 1982. Cell 3 is nearly full of solids and is
undergoing pre-closure steps. This cell is equipped with a LDS and a slimes drain. The LDS was
dry in 2014 and the slimes drain system will be monitored once dewatering begins. In 2014, Cell
3 received solid Mill waste and solid 11e.2 byproduct material from in situ recovery ("ISR")
facilities.
2.4 Cell4A
Cell 4A is a 40-acre impoundment built in 2008. This cell is equipped with a LDS and a slimes
drain. The slimes drain system will be monitored once dewatering begins. The LDS in Cell 4A
was sampled in 2014, as described below. In 2014, Cell 4A received solutions from the Mill
process, and solid tailings sands.
2.4 Cell4B
Cell 4B is a 40-acre impoundment built in 2011. It operates as an evaporation pond which
receives solutions only. Cell 4B is equipped with a LDS. In 2014, Cell 4B received fluid from
the Mill process. The LDS in Cell4B was sampled in 2014, as described below.
3.0 SAMPLING EVENTS AND SAMPLING METHODOLOGY
3.1 Sampling Events
Samples of solutions from tailings Cells 1, 3, 4A, and 4B, the Cell2 slimes drain and the Cell4A
and Cell 4B LDSs were collected on August 19, 2014. During review of the duplicate metals
data and gross alpha minus Rn and U ("gross alpha") data, quality problems were noted. The
Quality Assurance Manager ("QAM") contacted the laboratories and requested a data review and
subsequent reanalysis of several samples which were still within the method-specified holding
times. The reanalysis of the samples is discussed in Section 4.0 below.
In accordance with the Permit, DRC was notified of the August 19, 2014 sampling event and a
DRC representative was present for a part of the sampling. The DRC representative collected a
split aliquot of the Tailings Cell 2 slimes drain sample.
2
Maps showing the locations of the tailings and slimes drain and, when applicable, LDS sampling
locations are attached under Tab B. Table 1, included in the Tables Tab, provides an overview of
all tailings wastewater monitoring samples collected during the current period and includes the
sampling date, laboratory report date, and the work order/lab set ID associated with the analytical
data.
The Permit requires that the tailings wastewater samples be analyzed for the water quality
parameters listed in Table 2 of the Permit and SVOCs.
3.2 Field Data
Attached under Tab A are copies of all of the field data sheets recorded in association with the
annual tailings wastewater monitoring program. Sampling dates are listed in Table 1.
3.3 Sampling Methodology, Equipment and Decontamination Procedures
As noted in the DRC-approved Sampling Plan, Revision 2.1, dated July 30, 2012, field filtering
and preservation of metals and gross alpha sample aliquots was not completed due to safety
concerns associated with the filtering apparatus and the backpressure created by the increased
viscosity of these samples. The gross alpha and metals aliquots were filtered and preserved as
necessary by the analytical laboratory. It is important to note that field preservation of the
samples is to preclude biological growth and prevent the inorganic analytes from precipitating.
Based on past field data, the tailings, LDS and slimes drain samples are at a pH of 3.0 or less at
the time of collection without additional preservative. The addition of acidic preservatives in the
field would add minimal if any protection from biological growth or precipitation. The VOC
sample aliquots were preserved in the field.
3.3.1 Tailings Cells
Tailings fluid samples were collected at the tailings cell sampling stations shown on the Figures
in Tab B using a ladle as noted in the DRC-approved Sampling Plan, Section 3.1.2.
Disposable or dedicated sample ladles were used during this sampling event and, as such, rinsate
samples were not required.
3.3.2 Cell 2 Slimes Drain
Once a tailings cell has started the dewatering procedures, a sample will be collected from the
slimes drain system. At this time Cell 2 is the only slimes drain that requires sampling. The
location of the slimes drain for Cell 2 is shown in Tab B. While Cells 3, 4A and 4B are equipped
with slimes drain sample locations, the Cells are still active and the slimes drains will not be
pumped (and/or sampled) until dewatering operations have commenced.
The Cell 2 slimes drain, shown on the Figures in Tab B, was sampled using a disposable bailer as
noted in the DRC-approved Sampling Plan, Section 3.1.3.
3
Due to the use of disposable bailer, a rinsate sample was not required.
3.3.3 Cell 4A Leak Detection Systems
The Cell 4A LDS sample was collected from the sampling station shown on the Figures in Tab B
using a dedicated stainless steel bucket and ladle as noted in the DRC-approved Sampling Plan,
Section 3.2.1.
3.3.4 Cell 4B Leak Detection Systems
The Cell 4B LDS sample was collected from the sampling station shown on the Figures in Tab B
using a dedicated stainless steel bucket and ladle as noted in the DRC-approved Sampling Plan,
Section 3.2.1.
3.3.5 Cells 1, 2, 3,
The Cells 1, 2, 3 LDSs were not sampled during the 2014 sampling event because the systems
were dry.
3.4 Field QC Samples
The field Quality Control ("QC") samples generated during this sampling event included one
duplicate and one trip blank per shipment to each laboratory which received samples for VOCs.
The duplicate sample (Cell 65) was submitted blind to the analytical laboratory. As previously
stated, no rinsate blanks were collected during this sampling event as only dedicated or
disposable equipment was used for sample collection.
3.5 Laboratory Results
All analytical results were provided by one of the Mill's two contract analytical laboratories,
GEL Laboratories ("GEL") or Chemtech-Ford ("CTF").
The laboratories utilized during this investigation were certified under the Environmental Lab
Certification Program administered by the UDEQ Bureau of Lab Improvement for the analyses
they completed.
The analytical data as well as the laboratory Quality Assurance ("QA")/QC summaries are
included under Tab C.
4.0 QUALITY ASSURANCE AND DATA EVALUATION
The Permit requires that the annual tailings wastewater sampling program be conducted in
compliance with the requirements specified in the Mill's approved White Mesa Uranium Mill
Groundwater Monitoring Quality Assurance Plan ("QAP"), the approved Sampling Plan and the
4
Permit itself. To meet this requirement, the data validation completed for the tailings wastewater
sampling program and discussed in this Section utilized the requirements outlined in the QAP,
the Permit and the approved Sampling Plan as necessary. The Mill QAM performed a QA/QC
review to confirm compliance of the monitoring program with the requirements of the Permit,
the QAP, and the Sampling Plan. As required, data QA includes preparation and analysis of QC
samples in the field, review of field procedures, an analyte completeness review, and quality
control review of laboratory data methods and data. Identification of field QC samples that were
collected and analyzed is provided in Section 3.4 and 4.3.1. Discussion of adherence to the
Sampling Plan is provided in Section 4.1. Analytical completeness review results are provided
in Section 4.2. The steps and tests applied to check laboratory data QA/QC are discussed in
Section 4.3.
The analytical laboratories have provided summary reports of the analytical QA/QC
measurements necessary to maintain conformance with National Environmental Laboratory
Accreditation Conference ("NELAC") certification and reporting protocol. The analytical
laboratory QA/QC Summary Reports, including copies of the Chain of Custody forms for each
set of Analytical Results, follow the analytical results under Tab C. Results of review of the
laboratory QA/QC information are provided under Tab E and discussed in Section 4.3, below.
4.1 Adherence to Sampling Plan and Permit Requirements
On a review of adherence by Mill personnel to the QA/QC requirements, the QAM observed that
QAIQC requirements established in the Permit, the QAP, and the Sampling Plan were met, as
discussed below.
4.2 Analyte Completeness Review
All analyses required by the Permit Table 2 were completed. In addition, all tailings wastewater
samples were analyzed for SVOCs as required by the Permit.
4.3 Data Validation
The QAP and the Permit identify the data validation steps and data quality control checks
required for the tailings wastewater monitoring program. Consistent with these requirements, the
QAM performed the following evaluations: a field data QA/QC evaluation, a receipt temperature
check, a holding time check, an analytical method check, a reporting limit check, a trip blank
check, a QA/QC evaluation of sample duplicates, a gross alpha counting error evaluation and a
review of each laboratory's repmted QA/QC information. Each evaluation is discussed in the
following sections. Data check tables indicating the results of each test are provided under Tab
E.
5
4.3.1 Field Data QA/QC Evaluation
The QAM performs a review of all field recorded data to assess adherence with QAP, Permit,
and Sampling Plan requirements. The assessment involved review of the Field Data sheets.
Review of the Field Data Sheets noted that all requirements for field data collection were met.
4.3.2 Holding Time Evaluation
QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding
time checks are provided under Tab E. All samples were received and analyzed within the
required holding time.
4.3.3 Laboratory Receipt Temperature Check
Chain of Custody sheets were reviewed to confirm compliance with the Permit. Sample receipt
temperature checks are provided under Tab E. All samples were received within the required
temperature limit.
4.3.4 Analytical Method Check
The analytical methods reported by both laboratories were checked against the required methods
specified in the QAP. The review indicated that the tailings program samples were analyzed in
accordance with Table 1 of the QAP except for the ammonia analyses presented in Tab C.
A W AL, the Mill's usual laboratory suffered a catastrophic fire at their facility in July of 2014
and could not accept Mill samples during the third quarter of 2014. CTF was used for the 2014
tailings sampling program non-radiochemistry analyses. CTF does not have Utah certification
for the ammonia methods specified in the DRC-approved QAP; however, CTF does have Utah
certification for other ammonia methods. EFRI discussed a method variation with DRC prior to
the third quarter sampling events and DRC approved a method variation for ammonia on July 28,
2014 provided that all QAP required RLs could be met. CTF achieved the QAP required RLs
with the alternate ammonia method. The tailings program samples were analyzed in accordance
with Table 1 of the QAP or the alternate DRC-approved method. Analytical method check
results are provided in Tab E.
4.3.5 Reporting Limit Evaluation
All analytical method reporting limits reported by both laboratories were checked against the
reporting limits specified in the Permit. Section I.E.4 of the Permit requires the following
Reporting Limits:
"all water quality analyses reported shall have a minimum detection limit or reporting limit
that is less than or equal to the respective:
i. Ground Water Quality Standards concentrations defined in Table 2 of this Permit,
6
ii. For TDS, Sulfate, and Chloride, the Minimum Detection Limit for those
constituents for Tailing Cell wastewater monitoring will be as follows: 1,000 mg/L,
1,000 mg/L, and 1 mg/L, respectively, and
iii. Lower limits of quantitation for groundwater for semi-volatile organic compounds
listed in Table 2 of EPA Method 82700, Revision 4, dated February, 2007."
Reporting limit evaluations are provided in Tab E. All analytes were measured and reported to
the required reporting limits. Several sets of sample results had the reporting limit raised for at
least one analyte due to sample dilution. In all cases the reported value for the analyte was
higher than the increased detection limit.
4.3.6 Trip Blank Evaluation
All trip blank results were reviewed to identify any blank contamination. Trip blank evaluations
are provided in Tab E. All trip blank results associated with the samples were less than the
reporting limit for all VOCs.
4.3. 7 QA/QC Evaluation for Sample Duplicates
Section 9.1.4 a) of the QAP states that the relative percent difference (the "RPD") will be
calculated for the comparison of duplicate and original field samples. The QAP acceptance limits
for RPDs between the duplicate and original field sample is less than or equal to 20% unless the
measured results are less than 5 times the required detection limit. This standard is based on the
EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review,
February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for all duplicate
pairs for all analytes regardless of whether or not the reported concentrations are greater than 5
times the required detection limits; however, data will be considered noncompliant only when
the results are greater than 5 times the required detection limit and the RPD is greater than 20%.
RPDs are also only calculated when both the sample and the duplicate report a detection for any
given analyte. If only one of the pair reports a detection the RPD cannot be calculated. The
additional duplicate information is provided for information purposes.
During data review, it was noted that the metals results for sample pair Cell4NCell 65 showed
poor reproducibility. The QAM contacted CTF and requested a review of the data. The
laboratory investigation noted that there was a sample switch during sample preparation, which
resulted in the wrong sample data being reported as for the metals duplicate. Since the metals
samples were still within the method-specified holding times, the duplicate sample was
reanalyzed and the data re-reported. The reanalysis data showed better agreement with the
parent sample and the issue was considered resolved.
The uranium and zinc results for the duplicate sample, Cell 4NCell 65, did not meet the
duplicate comparability check with an RPD of 25% and 21% respectively. Per the QAP,
Revision 7 .2, and in response to requests from DRC, a separate corrective action for duplicate
RPDs outside of acceptance limits has been developed. The revised procedure for duplicate
7
results outside of acceptance limits was implemented for the uranium and zinc results in
duplicate pair Cell 4NCell 65. The corrective actions that were taken (on the reanalysis data) in
accordance with the revised procedure are as follows: the QA Manager contacted the Analytical
Laboratory and requested a review of the raw data to assure that there were no transcription
errors and the data were accurately reported. The laboratory noted that the data were accurate
and reported correctly. Reanalysis was not completed as the RPDs above the limit are likely due
to interferences caused by the matrix as discussed below.
There is no effect on the usability of the data due to the uranium and zinc duplicate results
exceeding the comparability criteria because the matrix of the sample solution caused the
noncompliance.
Results of the RPD test are provided under Tab E. The radiologic duplicates are discussed in
Section 4.3.8 below.
4.3.8 Radiologies Counting Error
Section 9.14 of the QAP requires that all gross alpha analysis reported with an activity equal to
or greater than the Groundwater Compliance Limit (the "GWCL") (for the tailings wastewater
samples the Groundwater Quality Standard (the "GWQS") will be used), shall have a counting
variance that is equal to or less than 20% of the reported activity concentration. An error term
may be greater than 20% of the reported activity concentration when the sum of the activity
concentration and error term is less than or equal to the GWQS.
Results of routine radiologic sample QC are provided under Tab E. All tailings wastewater
radiologic sample results met the counting error requirement.
Section 9 .1.4 of the QAP also requires a comparability check between the sample and field
duplicate sample results utilizing the formula provided below:
The original duplicate sample did not meet the duplicate comparability check specified in the
QAP. Results of the RPD test are provided under Tab E. Per QAP, Revision 7.2, and in response
to requests from DRC, a separate corrective action for duplicate RPDs outside of acceptance
limits has been developed and is documented in the revised QAP. The revised procedure for
duplicate results outside of acceptance limits was implemented for the gross alpha results in
duplicate pair Cell 4A LOS/Cell 65. The corrective actions that were taken in accordance with
the revised procedure are as follows: the QA Manager contacted the Analytical Laboratory and
requested a review of the raw data to assure that there were no transcription errors and the data
were accurately reported. The laboratory noted that the data were accurate and reported
correctly. Reanalysis was not completed as the RPDs above the limit are likely due to
interferences caused by the matrix as discussed below.
8
The lack of comparability of the gross alpha results is indicative of a matrix interference and
does not affect the usability of the data. Matrix interference is most likely caused by high
concentrations of TDS and other constituents in the sample.
4.3.9 Laboratory Matrix QC Evaluation
Section 9.2 of the QAP requires that the laboratory's QA/QC Manager check the following items
in developing data reports: (1) sample preparation information is correct and complete, (2)
analysis information is correct and complete, (3) appropriate analytical laboratory procedures are
followed, (4) analytical results are correct and complete, (5) QC samples are within established
control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical
requirements have been met, and (8) documentation is complete. In addition to other laboratory
checks described above, EFRI's QA Manager rechecks QC samples and blanks (items (5) and
(6)) to confirm that the percent recovery for spikes and the relative percent difference for spike
duplicates are within the method-specific required limits, or that the case narrative sufficiently
explains any deviation from these limits. Results of this quantitative check are provided under
Tab E. All lab QA/QC results from both CTF and GEL met these requirements. There were QC
results which did not meet laboratory established acceptance limits, as identified in Tab E and
described below.
A significant number of the tailings wastewater samples had the RL raised for multiple analytes
due to matrix interference and/or sample dilution. RL evaluations are discussed in Section 4.3.5.
The check samples included at least the following: a method blank, a laboratory control spike
("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the equivalent, where
applicable. It should be noted that:
• Laboratory fortified blanks are equivalent to LCSs.
• Laboratory reagent blanks are equivalent to method blanks.
• Post digestion spikes are equivalent to MSs.
• Post digestion spike duplicates are equivalent to MSDs.
• For method E900.1, used to determine gross alpha, a sample duplicate was used instead
ofaMSD.
All qualifiers, and the corresponding explanations reported in the QA/QC Summary Reports for
any of the check samples for any of the analytical methods were reviewed by the QAM.
The QAP Section 8.1.2 requires that a MS/MSD pair be analyzed with each analytical batch,
depending upon the analytical method requirements and/or method limitations. The QAP does
not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the
MS/MSD pair be prepared on EFRI samples only. Acceptance limits for MS/MSDs are set by
the laboratories. The review of the information provided by the laboratories in the data packages
verified that the QAP requirement to analyze a MS/MSD pair with each analytical batch was
met. While the QAP does not require it, the recoveries were reviewed for compliance with the
9
laboratory established acceptance limits. The QAP does not require this level of review and the
results of this review are provided for information only.
The information from the Laboratory QA/QC Summary Reports indicates that the MS/MSDs
recoveries and the associated RPDs for all tailings wastewater samples were within acceptable
laboratory limits for all regulated compounds except as indicated in Tab E. The recoveries and
RPDs which are outside of the laboratory established acceptance limits do not affect the quality
or usability of the data because the recoveries and RPDs outside of the acceptance limits are
indicative of matrix interference. The recoveries outside of acceptance limits reported in these
analyses were due to a matrix interference caused by high levels of metals and other inorganic
constituents. The QAP requirement to analyze a MS/MSD pair with each analytical batch was
met and as such the data are compliant with the QAP.
Eleven metals MS/MSD recoveries were not calculated because the analyte level in the natural
sample was 4 times greater than the spike level added by the laboratory. It is not possible to
calculate the MS/MSD recovery when the sample results are significantly higher than the spike
amount added. In effect, the sample results mask the spike results and the calculations are not
possible. There is no effect on the quality or usability of the data.
The QAP specifies that surrogate compounds shall be employed for all organic analyses, but the
QAP does not specify acceptance limits for surrogate recoveries. The analytical data associated
with the annual sampling met the requirement specified in the QAP. The information from the
Laboratory QA/QC Summary Reports indicates that the surrogate recoveries were within
acceptable laboratory limits for the surrogate compounds. The requirement in the QAP to
analyze surrogate compounds was met and the data are compliant with the QAP. Furthermore,
there are no QAP requirements for surrogate recoveries.
The information from the Laboratory QA/QC Summary Reports indicates that the LCS
recoveries for the quarterly samples were within acceptable laboratory limits for all LCS
compounds except as noted in Tab E. The laboratory noted that even though the LCS recovery
was outside of the lab control limits it was within Marginal Exceedance limit (± 4 standard
deviations of mean recovery) and the batch is considered to be in control based on recoveries of
other analytes. There is no effect on the quality or usability of the data because the method was
in control as indicated by the recovery in other analytes. Furthermore, there are no requirements
in the QAP for LCS recovery assessment.
The QAP Section 8.1.2 requires that each analytical batch shall be accompanied by a reagent
blank. Contamination detected in analysis of reagent blanks (method blank) will be used to
evaluate any analytical laboratory contamination of environmental samples. The QAP criteria
for method blanks states that nonconformance will exist when blanks are within an order of
magnitude of the sample results. Iron, calcium, magnesium, potassium, sodium, tin, zinc,
manganese and ammonia were reported the method blanks from CTF. The QAP criteria were
met for iron, calcium, magnesium, potassium, sodium, zinc, manganese and ammonia because
the method blank detections were not within an order of magnitude of the sample results. The
method blank detection for tin could not be assessed using the QAP criteria because tin was not
10
detected in any of the samples above the required RL. The tin detection in the method blank did
not affect the samples because there were no detections in the samples which indicates that there
were no false positives reported in the samples as a result of laboratory contamination. The QAP
requirement to analyze a method blank with each batch and evaluate the results has been
completed as required. Method blank results are included in Tab E.
4.3.10 Gross Alpha
During the QC review it was noted that the gross alpha samples were not filtered by GEL prior to
analysis as requested on the COC. The QAM contacted the laboratory and requested the samples
be filtered and reanalyzed. The laboratory filtered the samples and reanalyzed them. All
filtering and reanalysis were completed within the method-specified holding time of 6-months.
The corrected data are reported in Tab C.
5.0 HISTORIC DATA
The historic analytical data for the tailings wastewater sampling program are included in Tab D.
In addition, the minimum and maximum concentrations compiled in the Utah Division of
Radiation Control Groundwater Quality Discharge Permit, Statement of Basis for a Uranium
Mining Facility at White Mesa, South of Blanding, Utah, dated December 1, 2004 are included
in Tab D.
6.0 SUMMARY AND CONCLUSIONS
6.1 Cell1
Cell 1 solutions were acidic in nature with a laboratory pH of 1.3. As expected, the solutions
contained gross alpha, major ions, metals, and one SVOC. VOCs were not detected. Regarding
major ions, chloride, fluoride, magnesium, ammonia, potassium, sodium and sulfate were one to
three orders of magnitude greater in concentration than the other major ions. Metals exhibiting
the greatest concentration by at least one order of magnitude higher than the other metals
analyzed included arsenic, cadmium, chromium, cobalt, copper, iron, lead, manganese,
molybdenum, nickel, selenium, uranium, vanadium and zinc. An increase in the gross alpha
concentration was noted in the 2014 sample. This increase was likely due to the following
factors:
• During the June, July and August 2014 operating period, fresh water was not added to the
Mill process. Re-circulated tailings liquids were used for process water. The re-
circulated fluids were returned to the tailings system or evaporation ponds following use
in the Mill process. This use of re-circulated fluids contributed to the concentration of
the fluids in Cell 1.
• During the August 2013 through August 2014 period, the Mill's production was limited
resulting in less fresh water added to the Mill process and therefore to the cell. The
11
decrease in fresh water additions resulted in concentration of the existing fluids due to a
lack of dilution.
• Recent drought conditions resulted in less precipitation, less storm water, and less rain
water being placed in the cell. Drought conditions also result in increased evaporation.
These factors also contributed to concentration of cell fluids.
The fluid levels in Cell 1 dropped 8.16 inches between August 2013 and August 2014. The
decrease in fluid levels is further evidence that the increase in the gross alpha results is caused by
a lack of dilution and subsequent concentration.
With the exception of gross alpha, the concentrations reported in the 2014 sample remained
within historic ranges. It is important to note that not all constituents present in the tailings fluids
will exhibit the same behavior as a result of concentration of the tailings fluids and the increases
in constituent results will not be linear. The individual constituent results are greatly affected by
the matrix of the tailings fluids and each constituent will behave differently based on the matrix
interactions and the differing solubility properties of the constituent.
6.2 Cell3
Cell 3 solutions were acidic in nature, with a laboratory pH of 2.2. As expected, the solutions
contained gross alpha, major ions, and metals. SVOCs and VOCs were not detected. Regarding
major ions, chloride, fluoride, magnesium, ammonia, sodium and sulfate were generally one to
two orders of magnitude greater in concentration than the other major ions. Metals exhibiting the
greatest concentration by at least one order of magnitude greater than the other metals analyzed
included arsenic, cadmium, chromium, cobalt, copper, iron, lead, manganese, molybdenum,
nickel, selenium, uranium, vanadium and zinc. The gross alpha result decreased from the 2013
sample. When comparing the 2014 data to the 2013 sampling events, the concentrations of
major ions and metals reported in the 2014 sample decreased from the 2013 sample, most likely
due to the fact that Cell 3 is no longer used for the disposal of fluids in preparation for eventual
closure. Cell 3 solutions are limited to a finite pool area of less than ten percent of the cell
surface area. The lack of fluids placed in tailings Cell 3 allowed for evaporation and
crystallization/solidification/precipitation of the inorganic constituents present in the remaining
fluids present, thus reducing the concentration in the fluid sample.
6.3 Cell4A
Cell 4A solutions were acidic in nature, with a laboratory pH of 1.7. As expected, the solutions
contained gross alpha, major ions, metals. SVOCs and VOCs were not detected. Cell 4A fluid
exhibited the highest major ion concentrations for chloride, fluoride, magnesium, ammonia,
sodium and sulfate. The metals arsenic, cadmium, chromium, cobalt, copper, iron, lead,
manganese, molybdenum, nickel, selenium, uranium, vanadium and zinc were one or more
orders of magnitude greater than the other metals analyzed. An increase in the gross alpha
concentration was noted in the 2014 sample. This increase was likely due to the following
factors:
12
• During the June, July and August 2014 operating period, fresh water was not added to the
Mill process. Re-circulated tailings liquids were used for process water. The re-
circulated fluids were returned to the tailings system or evaporation ponds following use
in the Mill process. This use of re-circulated fluids contributed to the concentration of
the fluids in Cell 4A.
• During the August 2013 through August 2014 period, the Mill's production was limited
resulting in less fresh water added to the Mill process and therefore to the cell. The
decrease in fresh water additions resulted in concentration of the existing fluids due to a
lack of dilution.
• Recent drought conditions resulted in less precipitation, less storm water, and less rain
water being placed in the cell. Drought conditions also result in increased evaporation.
These factors also contributed to concentration of cell fluids.
The fluid levels in Cell 4A dropped 11.52 inches between August 2013 and August 2014. The
decrease in fluid levels is further evidence that the increase in the gross alpha results is caused by
a lack of dilution and subsequent concentration.
With the exception of gross alpha, the concentrations reported in the 2014 sample remained
within historic ranges. It is important to note that not all constituents present in the tailings fluids
will exhibit the same behavior as a result of concentration of the tailings fluids and the increases
in constituent results will not be linear. The individual constituent results are greatly affected by
the matrix of the tailings fluids and each constituent will behave differently based on the matrix
interactions and the differing solubility properties of the constituent.
Comparison of Cell 4A fluids to those of Cells 1, and 4B reveals that Cell 4A is similar in
composition and concentration ratios to the fluids in Cells 1, and 4B.
6.4 Ce114B
Cell 4B solutions were acidic in nature, with a laboratory pH of 1.6. As expected, the solutions
contained gross alpha, major ions, metals and two SVOCs. VOCs were not detected. Cell 4B
fluid exhibited the highest major ion concentrations for chloride, fluoride, magnesium, ammonia,
sodium and sulfate. The metals arsenic, cadmium, chromium, cobalt, copper, iron, lead,
manganese, molybdenum, nickel, selenium, uranium, vanadium and zinc were one or more
orders of magnitude greater than the other metals analyzed. An increase in the gross alpha
concentration was noted in the 2014 sample. This increase was likely due to the following
factors:
• During the June, July and August 2014 operating period, fresh water was not added to the
Mill process. Re-circulated tailings liquids were used for process water. The re-
circulated fluids were returned to the tailings system or evaporation ponds following use
in the Mill process. This use of re-circulated fluids contributed to the concentration of
the fluids in Cell 4B.
13
• During the August 2013 through August 2014 period, the Mill's production was limited
resulting in less fresh water added to the Mill process and therefore to the cell. The
decrease in fresh water additions resulted in concentration of the existing fluids due to a
lack of dilution.
• Recent drought conditions resulted in less precipitation, less storm water, and less rain
water being placed in the cell. Drought conditions also result in increased evaporation.
These factors also contributed to concentration of cell fluids.
The fluid levels in Cell 4B dropped 32.88 inches between August 2013 and August 2014. The
decrease in fluid levels is further evidence that the increase in the gross alpha results is caused by
a lack of dilution and subsequent concentration.
With the exception of gross alpha, the concentrations reported in the 2014 sample remained
within historic ranges. It is important to note that not all constituents present in the tailings fluids
will exhibit the same behavior as a result of concentration of the tailings fluids and the increases
in constituent results will not be linear. The individual constituent results are greatly affected by
the matrix of the tailings fluids and each constituent will behave differently based on the matrix
interactions and the differing solubility properties of the constituent.
Comparison of Cell 4B fluids to those of Cells 1, and 4A reveals that Cell 4B is similar in
composition and concentration ratios to the fluids in Cells 1, and 4A.
6.5 Cell 2 Slimes Drain
Cell 2 Slimes drain fluid was acidic in nature, with a laboratory pH of 3.1. As expected, the
solutions contained gross alpha, major ions, metals and two SVOCs. VOCs were not detected.
Major ions that were highest in concentration by one or more orders of magnitude included
chloride, magnesium, ammonia, sodium and sulfate. For metals, arsenic, cadmium, chromium,
cobalt, copper, iron, manganese, nickel, selenium, uranium, vanadium and zinc were at least one
order of magnitude greater in concentration than other metals analyzed. An increase in the gross
alpha concentration was noted in the 2014 sample. The gross alpha result increased but is the
same order of magnitude of the historic data. Overall, the concentrations reported in the 2014
sample remained approximately the same as the 2013 sample. Concentration changes noted are
within the analytical accuracy of the methods used for analysis.
6.6 Cells 3, 4A and 4B Slimes Drain
In accordance with the Permit, the slimes drains for Cell 3, 4A and 4B are not required to be
sampled until dewatering operations have begun. Cell 1 is an evaporation pond and does not
have a slimes drain.
14
6. 7 Cell 2 Leak Detection System
Consistent with the Permit, Cell 2 LDS was not sampled during the 2014 sampling event. The
Cell 2 LDS is now dry and covered to prevent precipitation inflow.
6.8 Cells 1 and 3 Leak Detection System
Consistent with the Permit, Cells 1 and 3 leak detection systems were not sampled during the
2014 sampling event because the systems were dry.
6.9 Cell 4A Leak Detection System
Cell 4A LDS solutions were acidic in nature, with a laboratory pH of 2.4. As expected, the
solutions contained gross alpha, major ions, metals and one VOC. SVOCs were not detected.
Cell 4A LDS fluid exhibited the highest major ion concentrations for chloride, fluoride,
magnesium, ammonia, sodium and sulfate. The metals arsenic, cadmium, chromium, cobalt,
copper, iron, manganese, molybdenum, nickel, selenium, uranium, vanadium and zinc were one
or more orders of magnitude greater than the other metals analyzed. An increase in the gross
alpha concentration was noted in the 2014 sample. The concentrations reported in the Cell 4A
LDS fluid are similar to the concentrations reported for the fluid in Cell 4A. Because the Cell
4A LDS fluids are from Cell 4A, the similarities in concentration are expected. The factors and
lack of dilution affecting the Cell 4A fluid concentrations will have the same impacts and overall
affects on the LDS fluid concentrations. Overall, the concentrations reported in the 2014 Cell
4A LDS sample increased slightly from the 2013 sample. Increases were due to concentration of
the Cell 4A fluids caused by a lack of dilution as discussed above.
6.10 Cell4B Leak Detection System
Cell 4B LDS solutions were acidic in nature, with a laboratory pH of 2.2. As expected, the
solutions contained gross alpha, major ions, metals and one VOC. SVOCs were not detected.
Cell 4B LDS fluid exhibited the highest major ion concentrations for chloride, magnesium,
ammonia, sodium and sulfate. The metals arsenic, cadmium, chromium, cobalt, copper, iron,
manganese, molybdenum, nickel, selenium, uranium, vanadium and zinc were one or more
orders of magnitude greater than the other metals analyzed. An increase in the gross alpha
concentration was noted in the 2014 sample. The concentrations reported in the Cell 4B LDS
fluid are similar to the concentrations reported for the fluid in Cell4B. Because the Cell4B LDS
fluids are from Cell 4B, the similarities in concentration are expected. The factors and lack of
dilution affecting the Cell 4B fluid concentrations will have the same impacts and overall affects
on the LDS fluid concentrations. Overall, the concentrations reported in the 2014 Cell 4B LDS
sample increased slightly from the 2012 sample (no sample was collected in 2013 because the
system was dry). Increases were due to concentration of the Cell 4B fluids caused by a lack of
dilution as discussed above.
15
6.11 Summary and Conclusions of Analytical Results
The metals arsenic, cadmium, chromium, cobalt, copper, iron, manganese, molybdenum, nickel,
selenium, uranium, vanadium and zinc were generally present in greatest concentration for all
samples. For major ions, chloride, fluoride, magnesium, ammonia, sodium, and sulfate were
predominant. Increases were noted for several metals and major anions as well as in the gross
alpha concentrations. The increased concentrations are indicative of a "concentration effect" and
provide information relative to the system as a whole. The individual constituent results are
greatly affected by the matrix of the tailings fluids and each constituent will behave differently
based on the matrix interactions and the differing solubility properties of the constituent.
The increase in concentrations was expected because less fresh water was used in the Mill
process and therefore less fresh water was added to the tailings fluids resulting in diminished
dilution and higher constituent concentrations. Evidence of the decreased water addition can be
seen in the significant drops in the fluid levels in Cells 1, 4A and 4B and the increased total
dissolved solids results for Cells 1, 4A and 4B Cell4A LDS and Cell4B LDS. Specifically, Cell
1 fluid levels decreased by 8.16 inches, Cell 4A fluid levels decreased by 11.52 inches and Cell
4B fluid levels decreased by 32.88 inches. Increased evaporation due to drought conditions also
contributed to the decrease in fluid levels. The decrease in fluid levels and increased evaporation
resulted in an increase in concentrations of certain constituents.
7.0 CORRECTIVE ACTION REPORT
No corrective action reports are required for the 2014 annual sampling event.
7.1 Assessment of Corrective Actions from Previous Period
No corrective action reports were required for the 2013 annual sampling event and as such there
is no assessment of previous actions necessary.
16
7.0 SIGNATURE AND CERTIFICATION
This-document was prepared by Energy Fuels Resources (USA) Inc. on November 24, 2014.
ENERGY FUELS RESOURCES (USA) INC.
By:
Scott A. Bakken
Director, Permitting & Environmental Affairs
17
Certification:
I certify, under penalty of law, that this document and all attachments were prepared
under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gather and evaluate the information submitted. Based on my inquiry of the
person or persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fine and imprisonment for knowing violations.
f'...r~----~
Scott A. Bakken
Director, Permitting & Environmental Affairs
Energy Fuels Resources (USA) Inc.
18
TABLES
Table 1 Summary of 2014 Tailings Cell Wastewater Monitoring
Location Sample Date of Laboratory Report Work Order
Date Number/Lab Set ID
Cell 1 Tailings Fluid 8/19/2014 GEL-9/19/2014 ( 1011412014) GEL-358469
CTF-9/15/2014 ( 10/1612014) CTF -1408830
Cell 2 Slimes Drain 8119/2014 GEL-9/19/2014 ( 1011412014) GEL-358469
CTF-9115/2014 ( 10/1612014) CTF-1408830
Cell 3 Tailings Fluid 8119/2014 GEL-9/19/2014 (10/1412014) GEL-358469
CTF-9/15/2014 ( 1011612014) CTF-1408830
Cell 4A Tailings Fluid 8/19/2014 GEL-9/19/2014 ( 1011412014) GEL-358469
CTF-9115/2014 ( 10/1612014) CTF-1408830
Cell4 LDS 8/19/2014 GEL-9119/2014 ( 1011412014) GEL-358469
CTF-9115/2014 (1011612014) CTF-1408830
Cell 4B Tailings Fluid 8/19/2014 GEL-9/19/2014 ( 1011412014) GEL-358469
CTF-9/15/2014 ( 10/16/2014) CTF-1408830
Cell65 8/19/2014 GEL-9119/2014 (10/1412014) GEL-358469
(Duplicate of Cell 4A CTF-9/15/2014 ( 10/16/2014) CTF -1408830
Tailings Fluid)
Notes:
GEL = GEL Laboratories, LLC
CTF = Chemtech-Ford Laboratories
Date in italics and parentheses reflects the date of the revised report. The reports were revised due to reanalysis of all or
part of the constituents due to laboratory enors noted during the data review. All reanalyses were completed within the
method-specified holding times.
INDEX OFT ABS
Tab A Tailings and Slimes Drain Field Sheets
Tab B Sample Location Figures
Tab C Laboratory Analytical Reports
Tab D Chemical and Radiological Summary Tables
Tab E Quality Assurance and Data Validation Tables
E-1 Holding Time Evaluation
E-2 Laboratory Receipt Temperature Check
E-3 Analytical Method Check
E-4 Reporting Limit Evaluation
E-5 Trip Blank Evaluation
E-6 QA/QC Evaluation for Sample Duplicates
E-7 Radiologies Counting Error
E-8 Laboratory Matrix QC Evaluation
Tab A
Tailings and Slimes Drain Field Sheets
Field Data Reco ·d-Tailings. LDS and Slimes Droin Sampling
Location: __,L_...f _.\_,._\ __._I _____ Sampling Personnel:
Is this a Slimes Drain? DYes ~o
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only):_~N~A..,.L_ ______ _
Weather Conditions at Time of Sampling: Pc~•+ \'/ L l 0 ..,yty
Field Parameter Measurements:
-pll )\
-Temperature (°C) -0"-L..l..-------------
Analytical Parameters/Sample Collection Method:
;,.,..A..
IE Yes DNa DYes D D 1.1! , ..
Nutrients ~Yes DNa o Yes rltNo D 0 ~ ,I
Other,Non t$l Yes DNo o Yes l}lNo 0 0 !il
Radiola ic.s H
Gross Alpha l!l Yes oNo DYes ~No D 0 lj! EL..
SVOCs Iii Yes oNo o Yes IS No D 0 F-.. """" Conductivity Yes DNo DYes r;il'No 0 D
QC Samples Associated with this Location:
D Rinsate Blank
D Duplicate
Duplicate Sample Name: -\.
Notes: A.-to .... c.A oo. ~:4, a..± ago,,. C: ... t .... -.T & ........... c:.r l c, ........ \:1 c a ,k,..c;rk,A. ~~~k..S
Wc.r-s t:o llcc.-t~ l!...t 0 8'15 Le.£+ .S jh ,_ c..± t?SI7.
Field Dntn Rc ordM Tailings, LDS and Slimes Drain Sampling
Location: ~e.l\ z. .. n;.-..q
Is this a Slimes Drain? ~Yes oNo
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only): _ _.3_.__=l......._ . .._l....,O..__ _____ _
Weathe1· Conditions at Time of Sampling: P 4-rt \y C..\ o r.J cA¥
Field Parameter Measurements:
-pH AlA
-Temperature (0 C) _ _,.,&:.=.-~A_.__ ___________ _
Analytical Parameters/Sample Collection Method:
-fa..J.
OJ Yes DNo DYes !2fNo 0 ~ D ~·
Nutrients ~Yes DNo DYes ~No 0 jg D ,.
Other.Non l)g Yes oNo DYes IE No 0 ISif D \' Radiolo ics
Gross Alpha DNo o Yes ®No 0 6il: D i;:~--.
SVOCs DNo DYes f211No 0 l5lt D £:.1-c...-..-:f: f .. n>l
Yes oNo DYes I!IJ No 0 ® 0 "
QC Samples Associated with this Location:
o Rinsate Blank
o Duplicate
Duplicate Sample Name:
Notes: A .......... ~a o.._ s•+c.... r...t o~ns . c .. c.tr, ..... ~ )c............,c.r 1 o,,....._ Hc. ..... ckr-.sa...._ prc.sc.-\ .
.S~(?\LS \&<-=rc.. t.ol\e.cd-~,~ o.)-CJ8'Z5 LcQt .$',±,: e..+ ~ 8<.40. h>e c..o spt.'f-
-)'~c.. \'""""f-lc.. \QLA.±;.:».., Lt..~\-si=\e:.. ""t OSiY~
Field Data Record" Tailing , LDS and Slimes Drnin Samplin.,
Location: __ c=-::· e=-l.._,l,__=3::..._ ___ Sampling Personnel: /Z4 r .. ;,.., Pc~l~.er:. Te~~ \-\e.> 1 \~ky
Is this a Slimes Drain? o Yes ~o
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes ouly):_""'.A/JG.,L.;A"'----------
Weatber Conditions at Time of Sampling:_...~.f..s<t...r=~±w\~yr-~'-=-\~o~u~J~v,_ ______ _
I Field Parameter Measurements:
-pH NA
-Temperature (°C) __ N<-.x....:.A__._ __________ _
Analytical Parameters/Sample Collection Method:
Notes: A r-;nu.eL 1'>/'-r , 1 ic o--t o [(13.,<; &c~r-.... ,., T ,.. .......... c:;.C .3 Du.=-I~, ... ~ .,so._ Al l f.t'uc.-."\-~
S~f lc 1 , . e-re c a il ''"te.A A:i-0 ttoe>, u.ft-sj±t.. cd· l)9!0.
reid Data Record" Tailings, LDS and Slimes Drain Sampling
Location: C:e.-l\ Y, A
Is this a Slimes Drain?
Sampling Personnel:___6.:.:!.. .. ,., ........ , IP----¥-t
DYes ~o
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only): _ ___.N'-"-'A'--'---------
Weather Conditions at Time of Sampling: P t:...r-+ \y c_l ovcJj..-------
Field Parameter Measurements:
-pH ;\JA
-Temperature (°C) _ __.e...:V:.-..<..A....:..-__________ _
Analytical Parameters/Sample Collection Method:
oNo 0 Yes ~No 0 0 {g
Nutrients ~Yes oNo o Yes fii:lNo D 0 ~
Other.Non rgJ Yes oNo o Yes 00 No 0 0 lj(l
Radiolo iC$
Gross Alpha IE Yes 0 No DYes ag:No 0 0
SVOCs ~Yes oNo DYes lliTNo D 0
Conductivity 29' Yes DNa DYes No D 0
QC Samples Associated with this Location:
o Rinsate Blank
~Duplicate
Duplicate Sample Name: ~e..\\ 6 5
,,
,,
,,
Notes: An·weA b.A.. s,'.\c a.+= 0911. {::eA.CU6l r" .......... ~r, Qc..a..o. ·pnsc;.,...J fP.c .S~l.A.fj
.Sii\."'(\(lr·S ••.>=c;.rc colltG.~,.J., e-.+-occz!i. Ldlt sdc A-+ £29:15
-~.:~rol
-~.,.~
Field Data ecord-Tailings, LDS and imcs Drnin Sampliug
Location: C:t.\\ !:lA LOS Sampling Personnel: &fetr;A 1 "JA..-..... e.e
Is this a Slimes Drain? ... Ye~
If this is a Slimes Drain, measure depth to wastewater immediately befon sampling.
DTW immediately before sampling (slimes only):_-'N'---=A:......L...--------
Weatber Conditions at Time of Sampling: Po.. rHy (, \oL>e_L
Field Parameter Measurements:
-pH A/A
-Temperature (0C) ~N~A(...;!..-..-----------
Analytical Parameters/Sample Collection Method:
DNo o Yes ®No D 0 ~
Nutrients ~Yes DNa DYes ~No D D Oil
Other .Non f1!Yes DNa o Yes ~No D 0 IB
Radiola ics
Gross Alpha IE Yes DNo o Yes ~No D 0
SVOCs !j!l Yes DNa DYes ()jlNo D 0
Conductivity Yes oNo DYes No D 0
QC Samples Associated with this Location:
D Rinsate Blank
o Duplicate
Duplicate Sample Name:
~or~
\(
,,
•l
Notes: Acr-,i. .. u (A {!),._ .S.• 'I c.. t..+ 09.56. (.-p..cro&, !Ac"-~c. Ou.c-f'I'<..{{'.A.+ eo ..$~ • .......,l·~·
~l~ s LYG-Cr c.oHt..c...te.A. 1:'.-t ot;!.lO MSlM.sU WaS pl"'"''" o.-1-.\-l-.J \p.;&-,J,·e .....
£.ifu.J,. r!.aJ..iG •. Ju! si-o..~4lo.s stu! bvct..~ \= et-t..l>S M!sLl,..,v6c.. +w.~ t.W.A. \4kl
h ~t:ll Sc......yk ~::>qft·k-,s, Le-~t ~lie... a..+ c;q.5C).
Fi~ld Data Record-Taillngs, LDS qnd SliruesDrnln Sam pling
Location: (. t 1 L Y S
Is this a Slimes Drain?
Sampling Personnel: &-~..-. ..... , r4we-..... er:
o Yes ~No
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only): __ #'-"-_A _______ _
Weather Conditions at Time of Sampling: ec .. r±\V'---'Lr.=LI~"""v~A~~r--------
Field Parameter Measurements:
-pH
-Temperature (0C) -~...L..:>.------------
Analytical Parameters/Sample Collection Method:
oNo 0 0 ~
oNo 0 0 £11
oNo 0 0 QG
oNo 0 0
oNo 0 0
oNo 0 0
QC Samples Associated with this Location:
o Rinsate Blank
o Duplicate
Duplicate Sample Name: ___________ _
-~o..-J
"
\(
Notes: Acc\ve.e&. CM... c!-i c. ,;\.:\-looz
Sa..,..._fLc:.-J wc.rc c 0 II e.c..-hA a. i=
(,..•M"t=i""' \ 4.,..-..r. QLA.., pce.J.:. ..... t eo..r: .$~\·~·
1 o '<L L-c:.r-t i de o.. ·f. 16'2o.
FieLd Data ecord~Tailings, LDS and Slimes Drain, Sampling
Location: ~ 1 ~us LiJS Sampling Personnel: 6-c...r-r~"', T,a.\6Ac;.c
Is this a Slimes Drain? DYes ~No
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only): __ '--Y.~A _______ _
Weather Conditions at Time of Sampling: (> A.r--t ly c \ t:J v J.y
Field Parameter Measurements:
-pH JVA
-Temperature (0C) _/V~:.....A-'--------------
Analytical Parameters/Sample Collection Method:
0 D
Nutrients DNa DYes [lJ No D D ~
Other Non ~Yes DNa o Yes qa No D D ~ ,,
Radiolo ics
Gross Alpha !$"Yes DNa o Yes ~No 0 D
SVOCs ~:»Yes DNa DYes mNo 0 D
Conductivity Yes DNa DYes No 0 D
QC Samples Associated with this Location:
D Rinsate Blank
D Duplicate
Duplicate Sample Name:
Field Data Record-' nilings, LDS an<l Slimes D rain Sampling
Location: -~C.::::..e-!=::::;..!l....~,( _ ___!,6~5"~--Sampling Personnel: 6~H-,· ......... 1 l e-. ........... .;,.r
Is this a Slimes Drain? o Yes ,~&No
If this is a Slimes Drain, measure depth to wastewater immediately before sampling.
DTW immediately before sampling (slimes only):_~#__...A_._ _______ _
Weather Conditions at Time of Sampling:. _ ___;P:.-<>--;......:_r-__.:.+-_\y.,__L=-:.1-':::o.=.v...:.vl-..:,Vr-_____ _
(
Field Parameter Measurements:
-pH ;VA
-Temperature (°C) _11/r:...=;_...;..A-=-------------
Analytical Parameters/Sample Collection Method:
t--f='"l'l
~Yes DNa DYes ~No D D ~ \\
Nutrients 1}11 Yes DNa o Yes ~No 0 0 ~ \\
Other.Non f$Yes oNo o Yes ~-No 0 0 ~ Radiolo ics '\
Gross Alpha ~Yes DNa DYes rENo 0 0 ~ 6EL
SVOCs ~Yes DNa DYes OCNo D 0 ~ C:..l-~T -l=u-~
Conductivity 19 Yes DNa o Yes No D 0 est '-'-
QC Samples Associated with this Location:
o Rinsate Blank
o Duplicate
Duplicate Sample Name:
Notes: Dve: l. c.:c.... ~ ~ (2{' ~-ll Gj_A.
TabB
Sample Location Figures
~ w "'
" " "' 0 Q_
(]> 3: -o
"' ~ ::J "' [.;:
t: 0 a. "' "' _!!)
~
0 :> c c 5 c Q) c "' "' 0 c 0 :::0
"' "' :§ ·c; >-./ "' c ·a._
a. 0 :::0 ./ ..J ..J ~ ./ ..c
B ::) ./ (},
::) ./ :ii
MW-02 •
32
MW-03 •
500'
-~-
' 0
II
II
tl
500'
SCALE: 1" •1,000'
CELL 1
1,000'
MW-17 •
33
PIEZ·2 u
PIEZ-3 •
OTW4·5
TW4·1 cPTW4•9
0 QTW4-3 OTW4-12
lbTW4-11 OTW4-13
TW4-~-8
OTW4-1
OTW4-4CTW4-14
OTW4-6
PIEZ-4
II
PIEZ-5 •
W Energy Fuels Resources (USA) Inc.
Author:
White Mesa Mfll
::itate: Utah
Annual Tailings
Sample Locations
Date: 10/8/14 Drafte<fBy:
-"' w
Q'
co " "' 0
(]._
'!' ·a f-
0 ::J c c ~ c "
I
I
t~
I
I
I
I
I
! ~-21
?
~ / ~r----.... ::u
MW·02 •
32
MW-03 •
500'
~~~
' 500' 1,000'
SCALE: 1" = 1,000'
CELL 1
LEAK
DETECTION
SAMPLE
LOCATION
MW·17 •
33
PJEZ-2
PIEZ-3 •
•
1 OlW4-13 TW4-~-8
OTW4·1
01W4-40TW4·14
OTW4·6
X
PIEZ-4 '1-';---~·-·.-.:-.. •
PIEZ·5 •
/ ~.,­.-/
'6fll: Energy Fuels Resources (USA) Inc.
REVISIONS
Date By
10/8/14 RE
Author:
White Mesa Mill
tate: Utah
Slimes and Leak Detection
Sample Locations
Date: 10/8/14 Drafted By:
TabC
Laboratory Analytical Reports
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 1
Comments:
Sample Matrix: Water
PO Number:
Parameter
Calculations
Anio~ Tn1al
Cation/ Anion Balance
Cations, Total
TDS Balance
lnor~:anic
AlkhliniJ.y-Dicarboual~ (HC03)
Alkalinity-Carbonate (C03)
AmmoniaasN
Chloride
Conductivity
Fluoride
Nitrate + Nitrite, Total
pH
Sulfate
Total Dissolved Solids (TDS)
TDS, Calculated
\1etals
Arseri.ic, Dissolved
Beryllium, Dissolved
Calcium, Dissolved
Cadmium, Dissolved
Cobalt, Dissolved
Chromium, Dissolved
Copper, Dissolved
Iron, Dissolved
Lead, Dissolved
Mercury, Dissolved
Magnesium, Dissolved
Manganese, Dissolved
Molybdenum, Dissolved
Nickel, Dissolved
Potassium, Dissolved
Selenium, Dissolved
Silver, Dissolved
Tin, Dissolved
Sodium, Dissolved
www chemtechford com
Main Report-no surr.rpt
Sample
Result
2910
-41
1220
92
ND
ND
5700
11600
113000
2380
53.0
1.3
124000
174000
159000
249
0.448
404
3.06
56.5
13.2
3420
2520
13.5
0.0125
5530
162
68.8
129
3010
3.97
0.336
ND
12200
Page 7 of90
Certificate of Analysis
Minimum
Reporting
Limlt
r.o
1.0
25.0
500
50.0
10.0
0.1
1000
1000
5
5.00
0.010
2.0
2.00
5.00
5.00
10.0
11.0
5.00
0.0020
2.0
0.800
5.00
5.00
5.0
0.0500
0.100
17.0
5.0
Units
meq/L
%
meq/L
%
mg!L
mg/L
mg/L
mg/L
umbo/em
mg/L
mg/L
pH Units
mg!L
mg!L
mg!L
mg/L
mg/L
mg/L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg/L
mg/L
mg/L
mg/L
mg/L
mgiL
mgiL
mg/L
mg/L
mgiL
Lab Sample No.: 1408830-01
Sample Date: 8/19/2014 8:15AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Analytical
Method
SM 1030E
SM 1030E
SM 1030E
SM2340B
SM2320B
SM2320B
SM 4500 NH3-D
EPA300.0
EPA120.1
EPA300.0
EPA353.2
SM4500H-B
EPA300.0
SM2540C
SM2540C
EPA200.8
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA245.1
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.7
Preparation
Date/Time
09/12/2014 12:47
09/12/2014 12:47
09/12/2014 12:47
09/12/2014 12:47
08/27/2014 10:00
08/27/2014 10:00
09/0112014 19:00
08/29/2014 17:00
08/22/2014 13:10
08/29/2014 17:00
09/04/2014 14:15
08/2112014 08:18
08/29/2014 17:00
08/2112014 13:32
09/12/2014 12:47
08/28/2014 10:16
08/25/2014 13:09
08/25/2014 13:09
08/28/2014 10:16
08/2812014 10:16
08/28/2014 10:16
08/28/2014 10:16
08/25/2014 13:09
08/28/2014 10:16
09/05/2014 16:11
08/25/2014 13:09
08/25/2014 13:09
08/28/2014 10:16
0812812014 10:16
08/25/2014 13:09
08/29/2014 11:05
08/2912014 II :05
08/2512014 13:09
08/25/2014 13:09
Analysis
Date/Time
9/12/2014 13:05
9/12/2014 13:05
9/12/2014 13:05
9/12/2014 14:28
8/28/2014 13:38
8/28/2014 13:38
911/2014 19:00
8/29/2014 17:00
8/25/2014 14:53
8/29/2014 17:00
9/4/2014 14:15
8/2112014 8:18
8/29/2014 17:00
8/2112014 13:32
9/12/2014 14:28
8/28/2014 14:53
8/25/2014 15:59
8/25/2014 15:59
8/28/2014 14:53
8/28/2014 14:53
8/28/2014 14:53
8/28/2014 14:53
8/25/2014 15:59
8/28/2014 14:53
9/812014 8:45
8/25/2014 15:59
8/25/2014 15:59
8/28/2014 14:53
8/28/2014 14:53
8/25/2014 15:59
8/29/2014 13:10
8/29/2014 13:10
8125/2014 15:59
8/25/2014 15:59
Flag
SPH
Page 3 of37 9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 1
Comments:
Sample Matrix: Water
PO Number:
Parameter
Metals
Thallium, Dissolved
Vanadium, Dissolved
Zinc, Dissolved
Radiochemistry
Ul'llniumJ Oi~Jvc:d
Semi-Volatile Compounds
1-Methylnaphthalene
l ,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitropheno1
2,4-Dinitroto1uene
2,6-Dinitrotoluene
2-Ch1oronaphthalene
2-Ch1orophenol
2-Methylnaphtha1ene
2-Methylpheno1
2-Nitrophenol
3 & 4-Methylphenol
3,3 '-Dich1orobenzidine
4-Chlorophenol
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylpheno1
4-Chlorophenyl Phenyl Ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzidine
www.chemlechlord.com
MainReport-no surr rpl
Sample
Result
0.876
485
229
137
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
41
Page 8 of90
Certificate of Analysis
Minimum
Reporting
Limit
0.0200
5.00
5.00
5:00
10
10
10
10
10
10
10
10
10
20
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units
mg/L
mg/L
mg/L
mg/L
ug/L
ug/L
ugiL
ugiL
ug/L
ugiL
ugiL
ugfL
ugiL
ug/L
ugiL
ugfL
ugfL
ugiL
ugiL
ug/L
ugfL
ugfL
ugiL
ugfL
ug/L
ug/L
ugfL
ugiL
ugfL
ugfL
ugiL
ugfL
ugiL
ugiL
Analytical
Method
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page4ol37
Lab Sample No.: 1408830-01
Sample Date: 8/19/2014 8:15AM
Receipt Date: 8/21/2014 8:30AM
Sampler: Gartin Palmer
Project: White Mesa Mill-Tailings
Project Number: White Mesa Mill-Groundwater
Preparation
Date/Time
08/29/2014 11:05
08/28/2014 10:16
08/25/2014 13:09
08/28/2014 10:16
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
Analysis
Date/Time
8/29/2014 13:10
8/28/2014 14:53
8/25/2014 15:59
8/28/2014 14:53
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:3 7
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:3 7
8/28/2014 0:3 7
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:3 7
8/28/2014 0:37
8/28/2014 0:37
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 1
Comments:
Sample Matrix: Water
PO Number:
Parameter
Semi-Volatile Compounds
Benzo ((I) llnthrncenu
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g,h,i) perylene
Benzo (k) fluoranthene
Bis (2-chloroethoxy) Methane
Bis (2-ch\oroethy\) Ether
Bis (2-chloroisopropy\) Ether
Bis (2-ethylhexy1) Phthalate
Buty1benzy\phthalate
Chrysene
Dibenzo (a,h) anthracene
Diethy1phthalate
Dimethyl phthalate
Di-n-butylphthalate
Di-n-Octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno (1,2,3-cd) pyrene
lsophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
WWii chemlechfO<d com
MainReport-no surr rpt
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
32
Page 9 of90
Certificate of Analysis
Minimum
Reporting
Limit
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units
ugll..
ug/L
ug!L
ug/L
ug/L
ug/L
ugiL
ugiL
ug/L
ug/L
ug/L
ug/L
ug!L
ugiL
ugiL
ug!L
ug!L
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ug/L
ugiL
ug/L
ugiL
ugiL
ug/L
ug/L
ug/L
Analytical
Method
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page 5of37
Lab Sample No.: 1408830-01
Sample Date: 8/19/2014 8:15AM
RecelptDate: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Daterrime
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08122/2014 07:52
08/22/2014 07:52
08/2212014 07:52
Analysis
Daterrime
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
8/28/2014 0:37
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
CHEMTECH-FORD
LABORATORIES
Name: Energy Fueh
Sample Site: Cell 1
Comments:
Sample Matrix: Water
PO Number:
Parameter
Volatile Organic Compounds
Acetone
Benzene
Carbon Tetrachloride
Chloroform
Chloromethane
Methyl Ethyl Ketone
Methylene Chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, total
www chemtechlord.com
MainReport-flO surr.rpt
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 10 of90
Certificate of Analysis
Minimum
Reporting
Limit
700
5.0
5.0
70.0
30.0
4000
5.0
100
46.0
1000
10000
Units
ug!L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Analytical
Method
aPA &2608
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
Page 6ol37
Lab Sample No.: 1408830-01
Sample Date: 8/19/2014 8:15AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Daterrlme
08/28/2014 18:24
08/28/2014 18:24
08/28/2014 18:24
08/28/2014 18:24
08/28/2014 18:24
08/28/2014 18:24
08/28/2014 18:24
08/28/2014 18:24
08/28/2014 18:24
08/28/2014 18:24
08/28/2014 18:24
Analysis
Datefl'ime
8/28/2014 18:24
8/28/2014 18:24
8/28/2014 18:24
8/28/2014 18:24
8/28/2014 18:24
8/28/2014 18:24
8/28/2014 18:24
8/28/2014 18:24
8/28/2014 18:24
8/28/2014 18:24
8/28/2014 18:24
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: October 14, 2014
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
SampleiD:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Celli
358469001
Ground Water
19-AUG-14 08:15
25-AUG-14
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Total Alpha Radium, Liquid "As Received"
Gross Radium Alpha 3.31E+05 +/-710
The following Analytical Methods were performed:
MDC
16.5
RL
1.00
----------------~~--Method Descrilili_on
EPA 900.1 Modified
Surrogate/Tracer Recovery Test
Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received"
Notes:
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
Project:
Client ID:
DNMIOOIOO
DNMIOOI
Units DF Analyst Date Time Batch Method
pCi/L CXP3 10/13/14 1538 1426429
Result Nominal Recovery% Acceptable Limits -----93.2 (25%-125%)
SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
the greater of either the adjusted MDL or the CRDL.
Page 12 of21
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 2 Slimes
Comments:
Sample Matrix: Water
PO Number:
Parameter
Calculations
Aoio~Tollll
Cation/Anion Balance
Cations, Total
TDSBalance
Inorganic
Alkalinity-.BicarMoare (HC03)
Alkalinity-Carbonate (C03)
AmmoniaasN
Chloride
Conductivity
Fluoride
Nitrate + Nitrite, Total
pH
Sulfate
Total Dissolved Solids (TDS)
TDS, Calculated
\leta Is
Arn<:D c, .Dll;solved
Becyllium, Dissolved
Calcium, Dissolved
Cadmium, Dissolved
Cobalt, Dissolved
Chromium, Dissolved
Copper, Dissolved
!ron, Dissolved
Lead, Dissolved
Mercury, Dissolved
Magnesium, Dissolved
Manganese, Dissolved
Molybdenum, Dissolved
Nickel, Dissolved
Potassium, Dissolved
Selenium, Dissolved
Silver, Dissolved
Tm, Dissolved
Sodium, Dissolved
www.dlemtechford.corn
Main Report-flO SUIT rpl
Sample
Result
1400
-47
511
86
ND
ND
3500
3720
54100
130
35.0
3.1
62200
87000
74900
19.8
0.197
322
6.48
46.7
1.63
126
2180
0.638
ND
2780
98.0
4.25
127
489
1.02
ND
ND
3130
Page 11 of 90
Certificate of Analysis
Minimum
Reporting
Limit
1.0
1.0
25.0
50
5.0
10.0
0.1
1000
1000
5
5.00
0.010
2.0
2.00
5.00
0.100
10.0
11.0
0.0500
0.0020
2.0
0.800
0.0500
5.00
5.0
0.0500
0.100
17.0
5.0
Units
roeqJt.
%
meq/L
%
mgiL
mg!L
mg!L
mg!L
umbo/em
mg!L
mg!L
pH Units
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mgiL
mg!L
mgiL
mg!L
mgiL
rng!L
mgiL
rng!L
mg!L
rng!L
Lab Sample No.: 1408830-02
Sample Date: 8/19/2014 8:25AM
RecelptDate: 8/21/2014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Analytical
Method
SM 1030E
SM 1030E
SM 1030E
SM2340B
SM 2320 B
SM2320B
SM 4500 NH3-D
EPA300.0
EPA 120.1
EPA300.0
EPA353.2
SM4500H-B
EPA300.0
SM2540 C
SM2540 C
EPA2QO.S
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA200.7
EPA200.8
EPA245.1
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.7
Preparation
Date/Time
O!lllV21}14 12:47
09112/2014 12:47
09/12/2014 12:47
09/12/2014 12:47
09/021201<1 00:00
09/02/2014 00:00
09/0112014 19:00
08/29/2014 17:00
08/22/2014 13:20
08/29/2014 17:00
09/04/2014 14:15
08/2112014 08:18
08/29/2014 17:00
08/2112014 13:32
09/12/2014 12:47
0812812014 10:16
08/25/2014 13:09
08/25/2014 13:09
08/28/2014 10:16
08/28/2014 10:16
08/25/2014 13:09
08/28/2014 10:16
08/25/2014 13:09
08/29/2014 11:05
09/05/2014 16:11
08/25/2014 13:09
08/25/2014 13:09
08/29/2014 11:05
08/28/2014 10:16
08/25/2014 13:09
08/29/2014 II :05
08/29/2014 11:05
08/25/2014 13:09
08/25/2014 13:09
Analysis
Date/Time
!1112n014 13:05
9/12/2014 13:05
9/12/2014 13:05
9/12/2014 14:28
9/212014 16:01
9/2/2014 16:01
9/2/2014 10:00
8/29/2014 17:00
8/22/2014 13:25
8/29/2014 17:00
9/4/2014 14:15
8/2112014 8:18
8/29/2014 17:00
8/2112014 13:32
911212014 14:28
812.8/2014 14:57
8/25/2014 16:06
8/25/2014 16:06
8/28/2014 14:57
8/28/2014 14:57
8/25/2014 16:06
8/28/2014 14:57
8/25/2014 16:06
8/29/2014 13:14
9/8/2014 8:45
8/25/2014 16:06
8/25/2014 16:06
8/29/2014 13:14
8/28/2014 14:57
8/25/2014 16:06
8/29/2014 13:14
8/29/2014 13:14
8125/2014 16:06
8/25/2014 16:06
Flag
SPH
Page 7ol 37 9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 2 Slimes
Comments:
Sample Matrix: Water
PO Number:
Parameter
Metals
TIIalll\Jill, D1$$0ived
Vanadium, Dissolved
Zinc, Dissolved
Radiochemistry
Uronium, Dl¥olved
Semi-Volatile Compounds
1-Metby lnaphtbaleue
1 ,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dicblorobenzene
1,4-Dichlorobenzene
2,4,5-Trichloropbenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylpbenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphtbalene
2-Cblorophenol
2-Metbylnaphtbalene
2-Methylphenol
2-Nitrophenol
3 & 4-Methylphenol
3,3 • -Dichlorobenzidine
4-Cblorophenol
4,6-Dinitro-2-metbylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-metbylphenol
4-Cblorophenyl Phenyl Ether
4-Nitrophenol
Acenaphthene
Acenaphtbylene
Antbrocene
Azobenzene
Benzidine
WNN chemtechford com
Main Report-no surr rpt
Sample
Result
0.402
497
405
11
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
11
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 12 of 90
Certificate of Analysis
Minimum
Reporting
Limit
0.0200
5.00
5.00
s.oo
10
10
10
10
10
10
10
10
10
20
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units
mg/L
mg/L
mg/L
mglt
ug!L
ug!L
ug/L
ug/L
ug!L
ug!L
ug/L
ug/L
ug!L
ug!L
ug/L
ug/L
ug/L
ug!L
ug/L
ug!L
ug!L
ug/L
ug/L
ug/L
ug/L
ug!L
ug!L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ugiL
Analytical
Method
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page 8 of37
Lab Sample No.: 1408830-02
Sample Date: 8/19/2014 8:25AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill-Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Datemme
08/29/2014 11:05
08/28/2014 10:16
08/25/2014 13:09
08/28/2014 10:16
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
Analysis
Datemme
8/29/2014 13:14
8/28/2014 14:57
8/25/2014 16:06
8/28/2014 14:57
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1 :03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1 :03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1 :03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1 :03
8/28/2014 1 :03
8/28/2014 1:03
8/28/2014 1:03
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 2 Slimes
Comments:
Sample Matrix: Water
PO Number:
Parameter
Semi-Volatile Compounds
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g,h,i) pery 1ene
Benzo (k) fluoranthene
Bis (2-cbloroethoxy) Methane
Bis (2-cbloroethyl) Ether
Bis (2-cbloroisopropyl) Ether
Bis (2-ethylhexyl) Phthalate
Butylbenzylphthalate
Cluysene
Dibenzo (a,h) anthracene
Diethylphthalate
Dimethyl phthalate
Di-n-butylphthalate
Di-n-Octylphthalate
Fluorauthene
Fluorene
Hexacblorobenzene
Hexacblorobutadiene
Hexacblorocyclopentadiene
Hexachloroethane
lndeno (1,2,3-cd) pyrene
lsophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
pyrene
Pyridine
WWN chemtechford com
MainReport-110 surr.rpt
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 13 of 90
Certificate of Analysis
Minimum
Reporting
Limit
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units
ug!L
ug!L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Analytical
Method
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page 9 of 37
Lab Samplo No.: 1408830-02
Sample Date: 8/19/2014 8:25AM
RecelptDate: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Date/Time
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
Analysis
Date/Time
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 I :03
8/28/2014 I :03
8/28/2014 I :03
8/28/2014 I :03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 I :03
8/28/2014 1:03
8/28/2014 1:03
8/28/2014 l :03
8/28/2014 1:03
8/28/2014 I :03
8/28/2014 I :03
8/28/2014 I :03
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
CHEMTECH-FORD
LABORATORIES
Name: Energy Fnels
Sample Site: Cell 2 Slimes
Comments:
Sample Matrix: Water
PO Number:
Parameter
Volatile Organic Compounds
Acetone
Benzene
Carbon Tetrachloride
Chloroform
Chloromethane
Methyl Ethyl Ketone
Methylene Chloride
Naphthalene
Tetrabydrofuran
Toluene
Xylenes, total
www chemtechlord oom
MainReport-flO surr.rpl
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 14 of90
Certificate of Analysis
Minimum
Reporting
Limit
700
5.0
5.0
70.0
30.0
4000
5.0
100
46.0
1000
10000
Units
ug/L
ug!L
ug/L
ug/L
ug/L
ug/L
ug/L
ug!L
ug!L
ug/L
ug/L
Analytical
Method
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
Page 10 of 37
Lab Sample No.: 1408830-02
Sample Date: 8/19/2014 8:25AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Date/Time
0812812014 18:41
08/28/2014 18:41
08/28/2014 18:41
08/28/2014 18:41
08/28/2014 18:41
08/28/2014 18:41
08/28/2014 18:41
08/28/2014 18:41
08/28/2014 18:41
08/28/2014 18:41
08/28/2014 18:41
Analysis
Datefl'ime
812812014 18:41
8/28/2014 18:41
8/28/2014 18:41
8/28/2014 18:41
8/28/2014 18:41
8/28/2014 18:41
8/28/2014 18:41
8/28/2014 18:41
8/28/2014 18:41
8/28/2014 18:41
8/28/2014 18:41
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone]-www.gel.com
Certificate of Analysis
Report Date: October 14, 2014
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Umon Boulevard
Parameter
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW -Cell 2 Slimes
358469002
Ground Water
19-AUG-14 08:25
25-AUG-14
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Total Alpha Radium, Liquid "As Received"
Gross Radium Alpha 6890 +/-98.1
The following Analytical Methods were performed:
Method Descri tion
EPA 900.1 Modified
Test ----
MDC
17.5
Surrogateffracer Recovery
Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received"
Notes:
Counting Uncertainty is calculated at the 68% confidence level (!-sigma).
RL
1.00
Result
Project:
Client ID;
DNMI00100
DNMIOOI
Units DF Analyst Date Time Batch Method
pCi/L CXP3 10/13/14 1537 1426429
Analvst Col!)_mems_
Nominal Recove % Acceptable Limits
101 (25%-125%)
SRL =Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
the greater of either the adjusted MDL or the CRDL.
Page 13 of21
CHEMTECH-FORD
LABORATORIES
Name: Energy Fnels
Sample Site: Cell 3
Comments:
Sample Matrix: Water
PO Number:
Parameter
Calculations
Anions, Total
Cation/ Anion Balance
Cations, Total
TDSBalance
Inorganic
Alkalinity -Bicarbonate (HC03)
Alkalinity-Carbonate (C03)
AmmoniaasN
Chloride
Conductivity
Fluoride
Nitrate +Nitrite, Total
pH
Sulfate
Total Dissolved Solids (TDS)
TDS, Calculated
Metals
Arsenic, Dissolved
Beryllium, Dissolved
Calcium, Dissolved
Cadmium, Dissolved
Cobalt, Dissolved
Chromium, Dissolved
Copper, Dissolved
Iron, Dissolved
Lead, Dissolved
Mercury, Dissolved
Magnesium, Dissolved
Manganese, Dissolved
Molybdenum, Dissolved
Nickel, Dissolved
Potassium, Dissolved
Selenium, Dissolved
Silver, Dissolved
Tm, Dissolved
Sodium, Dissolved
www chemtechford com
MainReport·no surr.rpt
Sample
Result
974
-44
377
73
ND
ND
3030
7200
56200
1330
59.5
2.2
37000
70100
51200
2.92
0.222
294
2.55
20.8
2.38
139
688
1.90
0.0024
1910
214
2.93
44.9
386
1.37
0.329
ND
3630
Page 15 of90
Certificate of Analysis
Minimum
Reporting
Limit
1.0
1.0
25.0
100
50.0
10.0
0.1
1000
1000
5
0.0500
0.010
2.0
2.00
5.00
0.100
10.0
11.0
0.0500
0.0020
2.0
0.800
0.0500
5.00
5.0
0.0500
0.100
17.0
5.0
Units
meq/L
%
meq/L
%
mg!L
mg!L
mg!L
mg!L
wnho/cm
mg!L
mg!L
pH Units
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
Lab Sample No.: 1408830-03
Sample Date: 8/19/2014 9:00AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Analytical
Method
SM 1030E
SM 1030E
SM 1030 E
SM2340B
SM2320B
SM2320B
SM 4500 NH3-D
EPA300.0
EPA120.1
EPA300.0
EPA353.2
SM4500H-B
EPA300.0
SM2540C
SM2540C
EPA200.8
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA200.7
EPA200.8
EPA245.1
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.7
Preparation
Date/Time
09/12/2014 12:47
09/12/2014 12:47
09/12/2014 12:47
09/12/2014 12:47
09/02/2014 00:00
09/02/2014 00:00
09/0112014 19:00
08/29/2014 17:00
08/22/2014 13:20
08/29/2014 17:00
09/04/2014 14:15
08/2112014 08:18
0812912014 17:00
08121/2014 13:32
09112/2014 12:47
08/29/2014 11:05
08/25/2014 13:13
08/25/2014 13:13
0812812014 10:16
0812812014 10:16
0812512014 13:13
0812812014 10:16
0812512014 13:13
08/29/2014 11:05
09/05/2014 16:11
08/25/2014 13: 13
08/2512014 13:13
08/29/2014 11:05
08/28/2014 10:16
08/2512014 13:13
08/29/2014 11:05
0812912014 11:05
08/25/2014 13:13
08/25/2014 13:13
Analysis
Date/Time
9/12/2014 13:05
9/12/2014 13:05
9/12/2014 13:05
9/12/2014 14:28
9/2/2014 16:01
9/2/2014 16:01
9/112014 19:00
8/29/2014 17:00
8/22/2014 13:25
8/29/2014 17:00
9/4/2014 14:15
812112014 8:18
812912014 17:00
812112014 13:32
9112/2014 14:28
8/2912014 13:17
8/2512014 16:24
8125/2014 16:24
812812014 15:00
812812014 15:00
812512014 16:24
812812014 15:00
8125/2014 16:24
8/29/2014 13:17
9/8/2014 8:45
8/2512014 16:24
8/25/2014 16:24
8/29/2014 13:17
8128/2014 15:00
8125/2014 16:24
8/29/2014 13:17
812912014 13:17
8/2512014 16:24
812512014 16:24
Flag
SPH
Page 11 of37 9632 South 500 West
Sandy. UT 84070
801-262-7299 Office
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 3
Comments:
Sample Matrix: Water
PO Number:
Parameter
\<leta Is
Thallium, Dissolved
Vanadium, Dissolved
Zinc, Dissolved
Radiochemistry
Uranium, Dissolved
Semi-Volatile Compounds
1-Methylnaphtbalene
1,2,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylpbenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Ch1orophenol
2-Methylnapbtha1ene
2-Methylpbenol
2-Nitropbeno1
3 & 4-Methy1phenol
3,3 '-Dichlorobenzidine
4-Chloropbenol
4,6-Dinitro-2-methylpbenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloropheny1 Phenyl Ether
4-Nitropheno1
Acenapbthene
Acenaphthylene
Anthracene
Azobenzene
Benzidine
www.chemlechford com
Main Report-flO SUIT rpl
Sample
Result
0.290
454
155
134
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 16 of90
Certificate of Analysis
Minimum
Reporting
Limit
0.0200
5.00
5.00
5.00
10
10
10
10
10
10
10
10
10
20
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
un1u
mgll..
mg/L
mg/L
mg/L
I! giL
ug/L
ug/L
ug!L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug!L
ug!L
ug/L
ug/L
ug/L
ug/L
ug!L
ug/L
ugiL
ug/L
ugiL
ug!L
ugiL
ugiL
Analytical
Method
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page 12 of 37
Lab Sample No.: 1408830~3
Sample Date: 8/19/2014 9:00AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Date/Time
0&/29120.t4. n :o.s
08/28/2014 10:16
08/25/2014 13:13
08/28/2014 10:16
0~2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08122/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
Analysis
Dateffime
8!29/iOJ4 11:17
8/28/2014 15:00
8/25/2014 16:24
8/2SI2014 15:00
812SI2ii14 1:30
8/28/2014 1:30
8/28/2014 I :30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
&128/2014 I :30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 I :30
8/28/2014 1:30
812812014 1:30
8/28/2014 1:30
8/2812014 1:30
8/2&12014 1:30
8/28/2014 1:30
8/28/2014 1:30
Flag
9632 South 500 West
Sandy, UT 84070
801·262-7299 Ofi'K:e
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 3
Comments:
Sample Matrix: Water
PO Number:
Parameter
Semi-Volatile Compounds
Benzo (II) Rnthn!Ccma
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g,h,i) pery1ene
Benzo (k) fluoranthene
Bis (2-<:hloroetboxy) Methane
Bis (2-<:hloroethyl) Ether
Bis (2-<:hloroisopropyl) Ether
Bis (2-ethylhexyl) Phthalate
Butylbenzy !phthalate
Chrysene
Dibenzo (a,h) anthracene
Diethylphthalate
Dimethyl phthalate
Di-n-butylphthalate
Di-n-Octylpbthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno (1,2,3-00) pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosodimetbylamille
N-Nitrosodi-n-propylamille
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyreoe
Pyridine
WNW dlemtechford com
MainReport-no surr.rpl
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 17 of 90
Certificate of Analysis
Minimum
Reporting
Limit
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units
ugfL
ug/L
ug/L
ugfL
ug!L
ug/L
ugfL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugfL
ugfL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugfL
ug/L
ugiL
ug!L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ugiL
Analytical
Method
EPAil270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page 13 of 37
Lab Sample No.: 1408830..()3
Sample Date: 8/19/2014 9:00AM
Receipt Date: 8/21/2014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Dateffime
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08122/2014 07:52
08/2212014 07:52
Analysis
Date/Time
8/28/2014 I :30
8/28/2014 I :30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 I :30
8/28/2014 I :30
8/28/2014 I :30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8128/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/20 14 1 :30
8/28/2014 1 :30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
8/28/2014 1:30
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 3
Comments:
Sample Matrix: Water
PO Number:
Parameter
Volatile Or~anic Compounds
Acetone
Benzene
Carbon Tetrachloride
Chloroform
Chloromethane
Methyl Ethyl Ketone
Methylene Chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, total
WWN chemtechford.oom
Main Report-no surr rpt
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 18 of 90
Certificate of Analysis
Minimum
Reporting
Limit
700
5.0
5.0
70.0
30.0
4000
5.0
100
46.0
1000
10000
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
Analytical
Method
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
Page 14 of 37
Lab Sample No.: 1408830-03
Sample Date: 8/19/2014 9:00AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Dateffime
08/28/2014 18:59
08/28/2014 18:59
08/28/2014 18:59
08/28/2014 18:59
08/28/2014 18:59
08/28/2014 18:59
08/28/2014 18:59
08/28/2014 18:59
08/28/2014 18:59
08/28/2014 18:59
08/28/2014 18:59
Analysis
Datetrime
8/28/2014 18:59
8/28/2014 18:59
8/28/2014 18:59
8/28/2014 18:59
8/28/2014 18:59
8/28/2014 18:59
8/28/2014 18:59
8/28/2014 18:59
8/28/2014 18:59
8/28/2014 18:59
8/28/2014 18:59
Flag
9632 South 500 West
Sandy, UT 64070
801-262-7299 Offoce
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone]-www.gel.com
Certificate of Analysis
Report Date: October 14, 2014
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Cell3
358469003
Ground Water
19-AUG-14 09:00
25-AUG-14
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Total Alpha Radium, Liquid "As Received"
Gross Radium Alpha 19700 +/-168
The following Analytical Methods were performed:
Method Description
EPA 900.1 Modified
Surrogate/Tracer Recovery Test
MDC
13.8
Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received"
Notes:
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
RL
1.00
Result
Project:
Client ID:
DNMIOOlOO
DNMIOOl
Units DF Analyst Date Time Batch Method ---
pCi/L CXP3 10/13/14 1537 1426429
Ana!yst Comments
Nominal Recovery% Acceptable Limi~s
102 (25%-125%)
SRL =Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
the greater of either the adjusted MDL or the CRDL.
Page 14 of21
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuel•
Sample Site: Cell4A
Comments:
Sample Matrix: Water
PO Number:
Parameter
Calculations
Anions, Total
Cation/ Anion Balance
Cations, Total
TDS Balance
lnor~anic
Alkalinity-Bicarbonate (HC03)
Alkalinity-Carbonate (C03)
AmmoniaasN
Chloride
Conductivity
Fluoride
Nitrate + Nitrite, Total
pH
Sulfate
Total Dissolved Solids (TDS)
TDS, Calculated
\leta Is
Arsenic, Dissolved
Beryllium, Dissolved
Calcium, Dissolved
Cadmium, Dissolved
Cobalt, Dissolved
Chromium, Dissolved
Copper, Dissolved
Iron, Dissolved
Lead, Dissolved
Mercury, Dissolved
Magnesium, Dissolved
Manganese, Dissolved
Molybdenum, Dissolved
Nickel, Dissolved
Potassium, Dissolved
Seleniwn, Dissolved
Silver, Dissolved
Ttn, Dissolved
Sodium, Dissolved
"""" O!m!b::l•lcrJ -
Main Report-no surr.rpt
Sample
Result
1520
-36
722
no
ND
ND
2730
5900
73000
1290
39.5
1.7
64900
97000
78300
70.0
0.190
445
1.78
27.5
4.62
556
2280
14.8
0.0025
2990
120
40.6
54.1
724
2.00
0.197
ND
7190
Page 19 of90
Certificate of Analysis
Minimum
Reporting
Limit
1.0
1.0
25.0
100
1
50.0
10.0
0.1
1000
1000
5
5.00
0.010
2.0
0.200
5.00
0.100
10.0
11.0
5.00
0.0020
2.0
0.800
5.00
5.00
5.0
0.500
0.100
17.0
5.0
Unlu
meqfL
%
meq/L
%
mg/L
mg/L
mg/L
mg/L
wnho/cm
mg/L
mg/L
pH Units
mg/L
mg/L
mg/L
rugiJ..
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mgiL
mg/L
mg/L
mg/L
Lab Sample No.: 1408830-04
Sample Date: 8/19/2014 9:25AM
Receipt Date: 8/21/2014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Analyttcal
Method
SM 1030 E
SM 1030E
SM 1030E
SM2340B
SM'2320B
SM2320B
SM 4500 NH3-D
EPA300.0
EPA 120.1
EPA300.0
EPA353.2
SM4500H-B
EPA300.0
SM2540C
SM2540C
EPA200.8
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA200.7
EPA200.8
EPA245.1
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.7
Preparation
Date/Time
09/1212014 12;47
09/12/2014 12:47
09/12/2014 12:47
09/12/2014 12:47
0910212014 00:00
09/02/2014 00:00
09/0112014 19:00
08/29/2014 17:00
08/22/2014 13:20
08/29/2014 17:00
09/04/2014 14:15
08/2112014 08:18
08/29/2014 17:00
08/2112014 13:32
09/12/2014 12:47
08/29/2014 ll :05
08/25/2014 13:13
08/25/2014 13:13
08/28/2014 10:16
08/28/2014 10:16
08/25/2014 13:13
08/28/2014 10:16
08/25/2014 13: 13
08/29/2014 ll :05
09/05/2014 16:1l
08/25/2014 13:13
08/25/2014 13:13
08/29/2014 ll :05
08/28/2014 10:16
08/25/2014 13: 13
08/29/2014 ll :05
08/29/20 14 11 :05
08/25/2014 13:13
08/25/2014 13:13
Analysis
Date/Time
10/16120-14 13:05
10/16/2014 13:05
10/16/2014 13:05
10/16/2014 14:28
9/2/2014 16:01
9/2/2014 16:01
9/l/2014 19:00
8/29/2014 17:00
8/22/2014 13:25
8/29/2014 17:00
9/4/2014 14:15
8/2112014 8:18
8/29/2014 17:00
8/21/2014 13:32
10/16/2014 14:28
10/9/2014 10:47
8/25/2014 16:28
8/25/2014 16:28
10/9/2014 ll:30
10/9/2014 10:47
10/10/2014 6:55
10/9/2014 10:47
10/10/2014 6:55
10/9/2014 10:47
9/8/2014 8:45
10/10/2014 6:55
10/10/2014 6:55
10/9/2014 10:47
10/9/2014 10:47
10/10/2014 6:55
10/9/2014 ll :30
10/9/2014 12:13
10/10/2014 6:55
10/10/2014 6:55
Flag
SPH
Page 15 of 37 9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 4A
Comments:
Sample Matrix: Water
PO Number:
Parameter
Metals
Thallium, Dissolved.
Vanadium, Dissolved
Zinc, Dissolved
Radiochemistry
Umnium1. DlsSol~c:d.
Semi-Volatile Compounds
l·MclflylnnpJlihalcne
1 ,2,4-Tricblorobenzene
1,2-Dicblorobenzene
1,3-Dich\orobeozene
I ,4-Dicblorobeozene
2,4,5-Tricblorophenol
2,4,6-Trichloropheool
2,4-Dichloropheool
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chlorooaphthalene
2-Chlorophenol
2-Methyloaphthalene
2-Methylphenol
2-Nitrophenol
3 & 4-Methylphenol
3,3 '-Dichtorobenzidioe
4-Chloropheool
4,6-Dioitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chlorophenyl Phenyl Ether
4-Nitropheool
Aceoaphthene
Aceoaphthyleoe
Anthracene
Azobeozene
Benzidine
www chemtechford com
MainReport-no surr.rpt
Sample
Result
0.376
535
169
159
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 20 of90
Certificate of Analysis
Minimum
Reporting
Limit
0.0200
5.00
5.00
5.00
10
10
10
10
10
10
10
10
10
20
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units
mg!L
mg!L
mg!L
mg!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ugfL
ug!L
ugfL
ug!L
ug!L
ug!L
ugfL
ug!L
ugfL
ug!L
ug!L
ugiL
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ugfL
ugfL
ugfL
ugfL
ugfL
ug!L
Analytical
Method
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page 16 of 37
Lab Sample No.: 1408830-04
Sample Date: 8/19/2014 9:25 AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Date/Time
0812912014 II :OS.
08/28/2014 10:16
08/25/2014 13: 13
08/28/2014 10:16
08/2212(114 07~52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
0812212014 07:52
0812212014 07:52
0812212014 07:52
08/2212014 07:52
08/2212014 07:52
Analysis
Date/Time
10/912014 12:13
10/9/2014 10:47
10/10/2014 6:55
10/9/2014 10:47
812812014 I ~5"6
8/28/2014 1:56
8/28/2014 I :56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 I :56
8/28/2014 I :56
8128/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 I :56
8/28/2014 1:56
8/28/2014 I :56
8/2812014 1:56
8/28/2014 1:56
812812014 1:56
8/28/2014 1:56
8/28/2014 1:56
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 OffiCe
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell4A
Comments:
Sample Matrix: Water
PO Number:
Parameter
Semi-Volatile Compounds
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g,h,i) perylene
Benzo (k) fluoranthene
Bis (2-chloroethoxy) Methane
Bis (2-chloroethyl) Ether
Bis (2-chloroisopropyl) Ether
Bis (2-ethylhexyl) Phthalate
Butylbenzylphthalate
Chrysene
Dibenzo (a,h) anthracene
Diethylphthalate
Dimethyl phthalate
Di-n-butylphthalate
Di-n-Octylphthalate
F1uoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno (1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
www .chemtechford com
Main Report-no surr rpt
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 21 of90
Certificate of Analysis
Minimum
Reporting
Limit
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ug/L
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ug/L
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ug/L
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
Analytical
Method
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page 17 of 37
Lab Sample No.: 1408830~4
Sample Date: 8/19/2014 9:25AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Dateffime
0812212014 O'h52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08122/2014 07:52
08/22/2014 07:52
Analysis
Daterrime
8/28120 14 I :~6
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 I :56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 I :56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 I :56
8/28/2014 I :56
8/28/2014 I :56
8/28/2014 I :56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8128/2014 1:56
8/28/2014 1:56
8/28/2014 1:56
8128/2014 1:56
Flag
9632 South 500 West
Sandy, UT 64070
801-262-7299 OffiCe
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 4A
Comments:
Sample Matrix: Water
PO Number:
Parameter
Volatile Organic Compounds
A<:4'10l}C
Benzene
Carbon Tetrachloride
Chloroform
Chloromethane
Methyl Ethyl Ketone
Methylene Chloride
Naphthalene
Tetrahydrofuran
Toluene
X ylenes, total
www.chemtechford com
MainReport-flo surr rpt
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 22 of90
Certificate of Analysis
Minimum
Reporting
Limit
700
5.0
5.0
70.0
30.0
4000
5.0
100
46.0
1000
10000
Unit!
og/1.
ug/1.
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
Analytical
Method
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
Page 18 of 37
Lab Sample No.: 1408830-04
Sample Date: 8/19/2014 9:25AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Date/Time
08/28/2014 19:17
08/28/2014 19:17
08/28/2014 19:17
08/28/2014 19:17
08/28/2014 19:17
08/28/2014 19:17
08/28/2014 19:17
08/28/2014 19:17
08/28/2014 19:17
08/28/2014 19:17
08/28/2014 19:17
Analysis
Date/Time
8/28/2014 19:17
8/28/2014 19:17
8/28/2014 19:17
8/28/2014 19:17
8/28/2014 19:17
8/28/2014 19:17
8/28/2014 19:17
8/28/2014 19:17
8/28/2014 19:17
8/28/2014 19:17
8/28/2014 19:17
Flag
9632 South 500 West
Sandy. UT 84070
801-262-7299 Office
GEL LAB ORA TORIES LLC
2040 Savage Road Charleston SC 29407-[phone]-www.gel.com
Certificate of Analysis
Report Date: October 14, 2014
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Celi4A
358469004
Ground Water
19-AUG-14 09:25
25-AUG-14
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Total Alpha Radium, Liquid "As Received"
Gross Radium Alpha 2.40E+05 +/-577
The following Analytical Methods were performed:
Method Description
EPA 900.1 Modified
Surrogate/Tracer Recover_y__ Test
MDC
13.6
Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received"
Notes:
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
RL
Project:
Client ID:
DNMIOOIOO
DNMIOOI
Units DF Analyst Date Time Batch Method
1.00 pCi/L CXP3 10/13/14 1537 1426429
t Comments
Result Nominal Recove % Acceptable Limits
101 (25%-125%)
SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
the greater of either the adjusted MDL or the CRDL.
Page 15 of21
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 4A LOS
Comments:
Sample Matrix: Water
PO Number:
Parameter
Calculations
Anions, Total
Cation/ Anion Balance
Cations, Total
TDS Balance
Inorganic
Alkalinity -Bicarbonate (HC03)
Alkalinity-Carbonate (C03)
AmmoniaasN
Chloride
Conductivity
Fluoride
Nitrate+ Nitrite, Total
pH
Sulfate
Total Dissolved Solids (TDS)
TDS, Calculated
Metals
Arsenic, Dissolved
Beryllium, Dissolved
Calcium, Dissolved
Cadmium, Dissolved
Cobalt, Dissolved
Cbromium, Dissolved
Copper, Dissolved
Iron, Dissolved
Lead, Dissolved
Mercury, Dissolved
Magnesium, Dissolved
Manganese, Dissolved
Molybdenum, Dissolved
Nickel, Dissolved
Potassium, Dissolved
Selenium, Dissolved
Silver, Dissolved
Tm, Dissolved
Sodium, Dissolved
www chemtechford rom
MainReport-no surr rpt
Sample
Result
1280
-42
530
85
ND
ND
2920
4200
53600
1320
39.0
2.4
56000
81900
69700
51.2
0.185
336
4.72
41.2
2.78
439
1850
0.991
ND
2690
98.6
3.97
99.3
415
2.17
ND
ND
4190
Page 23 of90
Certificate of Analysis
Minimum
Reporting
Limit
1.0
1.0
25.0
100
50.0
10.0
0.1
1000
1000
5
5.00
0.010
2.0
2.00
5.00
0.100
10.0
11.0
0.0500
0.0020
2.0
0.800
0.0500
5.00
5.0
0.0500
0.100
17.0
5.0
Units
mcq/L
%
meq/L
%
lllg/l.
mg/L
mg/L
mg/L
umbo/em
mg/L
mg/L
pH Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mgiL
mg/L
mg/L
mg/L
mg/L
mgiL
mg/L
mg/L
mg/L
mg/L
mg/L
Lab Sample No.: 1408830-45
Sample Date: 8/19/2014 9:40AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Analytical
Method
SM 1030 E
SM 1030E
SM 1030E
SM2340B
SM2J20 B
SM2320B
SM 4500 NH3-D
EPA300.0
EPA 120.1
EPA300.0
EPA353.2
SM4500H-B
EPA300.0
SM2540C
SM2540C
ePA200.8
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA200.7
EPA200.8
EPA245.l
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.7
Preparation
Date/flme
09112/2014 12:47
09/12/2014 12:47
09/12/2014 12:47
09/12/2014 12:47
o9romoJ4 .oo:oo
09/02/2014 00:00
09/01/2014 19:00
08/29/2014 17:00
08/22/2014 13:20
08/29/2014 17:00
09/04/2014 14:15
08/2112014 08:18
08/29/2014 17:00
08/2112014 13:32
09/12/2014 12:47
08/28/2014 10:16
08/25/2014 13:13
08/25/2014 13:13
08/28/2014 10:16
08/28/2014 10:16
08/25/2014 13:13
08/28/2014 10:16
08/25/2014 13:13
08/29/2014 11:05
09/05/2014 16:11
08/25/2014 13:13
08/25/2014 13:13
08/29/2014 11:05
08/28/2014 10:16
08/25/2014 13:13
08/29/2014 11 :05
08/29/2014 11:05
08/25/2014 13:13
08/25/2014 13:13
Analysis
Dateffime
9112/.2014 13:05
9/12/2014 13:05
9/12/2014 13:05
9/12/2014 14:28
9/;V2()14 16:01
9/2/2014 16:01
9/1/2014 19:00
8/29/2014 17:00
8/22/2014 13:25
8/29/2014 17:00
9/4/2014 14:15
8/2112014 8:18
8/29/2014 17:00
8/2112014 13:32
9/12/2014 14:28
8/28/2014 15:19
8/25/2014 16:32
8/25/2014 16:32
8/28/2014 15:19
8/28/2014 15:19
8/25/2014 16:32
8/28/2014 15:19
8/25/2014 16:32
8/29/2014 13:24
9/8/2014 8:45
8/25/2014 16:32
8/25/2014 16:32
8/29/2014 13:24
8/28/2014 15:19
8/25/2014 16:32
8/29/2014 13:24
8/29/2014 13:24
8/25/2014 16:32
8/25/2014 16:32
Flag
SPH
Page 19 of37 9632 South 500 West
Sandy. UT 84070
801-262-7299 OffiCe
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 4A LDS
Comments:
Sample Matrix: Water
PO Number:
Parameter
Metals
1J1alliom. Dissolved
Vanadium, Dissolved
Zinc, Dissolved
Radiochemistry
Uranium, Dissolved
Semi-Volatile Compounds
1-MclllylnnphtMI,cnc
I ,2,4-Trichlorobenzene
I ,2-Dichlorobenzene
1,3-Dichlorobenzene
I ,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichloropheno1
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitroto1uene
2-Chloronaphtha1ene
2-Chlorophenol
2-Methylnaphthalene
2-Methylpheno\
2-Nitrophenol
3 & 4-Methylpheno\
3,3 '-Dichlorobenzidine
4-Chloropheno\
4,6-Dinitro-2-methylphenol
4-Bromopheny1 phenyl ether
4-Ch1oro-3-methylphenol
4-Ch1oropheny1 Phenyl Ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzidine
www chemtechford rom
Main Report-no SUIT rpl
Sample
Result
0.522
510
306
82.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 24 of90
Certificate of Analysis
Minimum
Reporting
Limit
0.0200
5.00
5.00
5.00
10
10
10
10
10
10
10
10
10
20
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units
mg!L
mg!L
mg!L
mg!L
ug/L
ug/L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
Analytical
Method
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page 20 of 37
Lab Sample No.: 1408830-05
Sample Date: 8/19/2014 9:40AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill-Groundwater
Preparation
Date/Time
08/29/2014 11:05
08/28/2014 10:16
08/25/20 14 13: 13
08/28/2014 10:16
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
Analysis
Date/Time
8/29/2014 13:24
8/28/2014 15:19
8/25/2014 16:32
8/28/2014 15:19
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8128/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/2812014 2:22
8128/2014 2:22
8/2812014 2:22
8128/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8128/2014 2:22
8/2812014 2:22
8/28/2014 2:22
8128/2014 2:22
8128/2014 2:22
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 4A LDS
Comments:
Sample Matrix: Water
PO Number:
Parameter
Semi-Volatile Compounds
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g,h,i) perylene
Benzo (k) fluoranthene
Bis (2-chloroethoxy) Methane
Bis (2-chloroethyl) Ether
Bis (2-chloroisopropyl) Ether
Bis (2-ethylhexyl) Phthalate
Butylbenzylphthalate
Chrysene
Dibenzo (a,h) anthracene
Diethylphlhalate
Dimethyl phthalate
Di-n-butylphthalate
Di-n-Octylphlhalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno (1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
www chemtechlord.com
Main Report-no SUIT rpl
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 25 of90
Certificate of Analysis
Minimum
Reporting
Limit
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
Analytleal
Method
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page21 of37
Lab Sample No.: 1408830-05
Sample Date: 8/19/2014 9:40AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill-Groundwater
Preparation
Date/Time
08/2212o 14 on52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
Analysis
Date/Time
S/2812014 2:'22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
8/28/2014 2:22
Flag
9632 South 500 West
Sandy UT 84070
801-262-7299 OffiCe
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 4A LDS
Comments:
Sample Matrix: Water
PO Number:
Parameter
Volatile Organic Compounds
Acetone
Benzene
Carbon Tetrachloride
Chloroform
Chloromethane
Methyl Ethyl Ketone
Methylene Chloride
Naphthalene
Tetrahydrofuran
Toluene
X ylenes, total
www chemtecllford rom
Main Report-no surr rpt
Sample
Result
ND
ND
ND
95.0
ND
ND
ND
ND
ND
ND
ND
Page 26 of90
Certificate of Analysis
Minimum
Reporting
Limit
700
5.0
5.0
70.0
30.0
4000
5.0
100
46.0
1000
10000
Units
ug/L
ug!L
ug/L
ug/L
ug/L
ug/L
ug/L
ug!L
ug/L
ugfL
ug/L
Analytical
Method
llPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
Page 22 of 37
Lab Sample No.: 1408830..05
Sample Date: 8/19/2014 9:40AM
Receipt Date: 8/21/2014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill-Tailings
Project Number: White Mesa Mill-Groundwater
Preparation
DaWTime
0812812014 19:35
08/28/2014 19:35
08/28/2014 19:35
08/28/2014 19:35
08/28/2014 19:35
08/28/2014 19:35
08/28/2014 19:35
08/28/2014 19:35
08/28/2014 19:35
08/28/2014 19:35
08/28/2014 19:35
Analysis
Date/Time
812812014 I !l;3S
8/28/2014 19:35
8/28/2014 19:35
8/28/2014 19:35
8/28/2014 19:35
8/28/2014 19:35
8/28/2014 19:35
8/28/2014 19:35
8/28/2014 19:35
8/28/2014 19:35
8/28/2014 19:35
Flag
9632 South 500 West
Sandy, lJT 84070
801-262-7299 OffiCe
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Cell 4A LDS
358469005
Ground Water
19-AUG-14 09:40
25-AUG-14
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Total Alpha Radium, Liquid "As Received"
Gross Radium Alpha 61800 +/-289
MDC
13.1
The following Analytical Methods were performed: ~--------------
Method Descrii:J""'ti:.::.on:.:._.,=----
EPA 900.1 Modified
Surrogate/Tracer Recovery Test
Barium CatTier GFPC, Total Alpha Radium, Liquid "As Received"
Notes:
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
RL
1.00
Result
Project:
Client ID:
Report Date: October 14, 2014
DNMIOOlOO
DNMIOOl
Units DF Analyst Date Time Batch Method
pCi/L CXP3 10113/14 1537 1426429
Analyst Comments
Nominal _!{~covery% Acceptable Limits
103 (25%-125%)
SRL =Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
the greater of either the adjusted MDL or the CRDL.
Page 16 of21
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell4B
Comments:
Sample Matrix: Water
PO Number:
Parameter
Calculations
Anions, To!tll
Cation/Anion Balance
Cations, Total
TDS Balance
Inorganic
Alkalinity-Biettrbonilu: (liC03)
Alkalinity -Carbonate (C03)
AmmoniaasN
Chloride
Conductivity
Fluoride
Nitrate +Nitrite, Total
pH
Sulfate
Total Dissolved Solids (TDS)
IDS, Calculated
:vtetals
Arsenio, Dissa)verl.
Beryllium, Dissolved
Calcium, Dissolved
Cadmium, Dissolved
Cobalt, Dissolved
Chromium, Dissolved
Copper, Dissolved
Iron, Dissolved
Lead, Dissolved
Mercury, Dissolved
Magnesium, Dissolved
Manganese, Dissolved
Molybdenum, Dissolved
Nickel, Dissolved
Potassium, Dissolved
Selenium, Dissolved
Silver, Dissolved
Tm, Dissolved
Sodium, Dissolved
www chemtechford.oom
MainReport-110 surr rpt
Sample
Result
2110
-47
758
86
ND
ND
5380
7300
90100
1150
47.0
1.6
91500
131000
113000
70.4
0.275
366
2.29
24.6
6.94
368
2480
10.9
ND
3310
129
29.0
42.0
989
5.01
0.142
ND
7100
Page 27 of90
Certificate of Analysis
Minimum
Reporting
Limit
1.0
1.0
25.0
100
I
50.0
10.0
0.1
1000
1000
5
5.00
0.010
2.0
2.00
5.00
5.00
10.0
11.0
5.00
0.0020
2.0
0.800
5.00
5.00
5.0
0.0500
0.100
17.0
5.0
Units
meq/L
%
meq/L
%
mg/L
mg/L
mg/L
mg/L
wnholcm
mg/L
mg/L
pH Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg!L
mg/L
mg/L
mg/L
mg/L
mg/L
mg!L
mg/L
Lab Sample No.: 1408830..06
Sample Date: 8/19/2014 10:10 AM
Receipt Date: 8/21/2014 8:30AM
Sampler: Garrio Palmer
Project: White Mesa Mill-Tailings
Project Number: White Mesa Mill -Groundwater
Analytical
Method
SM 1030E
SM 1030E
SMI030E
SM2340B
SM2320B
SM2320B
SM 4500 NH3-D
EPA300.0
EPA120.1
EPA300.0
EPA353.2
SM4500H-B
EPA300.0
SM2540C
SM2540C
EPA200.8
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA245.l
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.7
Preparation
Daterrlme
0911212014 12:47
0911212014 12:47
0911212014 12:47
0911212014 12:47
09/0212014 00:00
09/0212014 00:00
09/0112014 19:00
0812912014 17:00
08/2212014 13:20
08/2912014 17:00
09104/2014 14:15
0812112014 08:18
0812912014 17:00
0812112014 13:32
09/1212014 12:47
08/28/2014 10:16
08/25/2014 13:13
08/25/2014 13:13
08/2812014 10:16
0812812014 10:16
08/28/2014 10:16
08/28/2014 10:16
08125/2014 13:13
08/28/2014 10:16
09/0512014 16: ll
08/25/2014 13:13
08/25/2014 13:13
08/28/2014 10:16
08/28/2014 10:16
08/25/2014 13:13
08/29/2014 11:05
08/2912014 11:05
08/25/2014 13:13
08/25/2014 13:13
Analy1u
Date/Time
9/12f2PI4 13~05
9/1212014 13:05
9/1212014 13:05
911212014 14:28
!)1212014 16·:0 I
9/212014 16:01
91112014 19:00
8/29/2014 17:00
8/2212014 13:25
8129/2014 17:00
9/412014 14:15
812112014 8:18
812912014 17:00
8/2112014 13:32
9/1212014 14:28
8/28/2014 15:2.6
8/25/2014 16:44
8/25/2014 16:44
8/2812014 15:26
812812014 15:26
812812014 15:26
8/28/2014 15:26
8/25/2014 16:44
8/28/2014 15:26
9/8/2014 8:45
8/2512014 16:44
8/25/2014 16:44
8/28/2014 15:26
8/28/2014 15:26
8/25/2014 16:44
8/29/2014 13:32
8/29/2014 13:32
8/2512014 16:44
8/25/2014 16:44
Flag
SPH
Page 23 of 37 9632 Soulh 500 West
Sandy, UT 64070
801-262-7299 Olfoce
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell4B
Comments:
Sample Matrix: Water
PO Number:
Parameter
:Vtetals
Tballiwn, Dissolved
Vanadiwn, Dissolved
Zinc, Dissolved
l{adiochemistry
Urimlwn, Pis. olv.!d
Semi-Volatile Compounds
1-Methylnaphthalene
I ,2,4-Trichlorobenzene
1 ,2-Dichlorobenzene
1,3-Dichlorobenzene
1 ,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3 & 4-Methylphenol
3,3 • -Dichlorobenzidine
4-Chlorophenol
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chlorophenyl Phenyl Ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzidine
www.chemtechford com
MalnReport-<10 surupl
Sample
Result
0.258
666
144
133
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
26
Page28 of90
Certificate of Analysis
Minimum
Reporting
Limit
0.0200
5.00
5.00
5.00
10
10
10
10
10
10
10
10
10
20
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units
ntg/L
mg!L
mg/L
m~
u8fL
ug!L
ug!L
ug!L
ug!L
ug/L
ug/L
ug/L
ug!L
ug/L
ug!L
ug!L
ugiL
ug!L
ug!L
ugiL
ug!L
ugiL
ugiL
ugiL
ug!L
ug!L
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ug!L
Analytleal
Method
llPA 200.8
EPA200.8
EPA200.7
EPA200.8
EPAS270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page 24 of37
Lab Sample No.: 1408830-06
Sample Date: 8/19/2014 I 0:10AM
Receipt Date: 8/21/2014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Date/Time
08/29/2014 11:05
08/28/2014 10:16
08/25/2014 13:13
(1812&!20 14 10: 16
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08122/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
Analysis
Date/Time
8/29/2014 13:32
8/28/2014 15:26
8/25/2014 16:44
&!2812014 15:26
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8128/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8128/2014 2:48
8128/2014 2:48
8128/2014 2:48
8/28/2014 2:48
8/2812014 2:48
Flag
9632 South 500 We~
Sandy, UT 84070
801-262-7299 Ofllce
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 4B
Comments:
Sample Matrix: Water
PO Number:
Parameter
Semi-Volatile Compounds
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g,h,i) perylene
Benzo (k) fluoranthene
Bis (2-chloroethoxy) Methane
Bis (2-chloroethyl) Ether
Bis (2-chloroisopropyl) Ether
Bis (2-ethylhexyl) Phthalate
Butylbenzylphthalate
Chrysene
Dibenzo (a,h) anthracene
Diethylphthalate
Dimethyl phthalate
Di-n-butylphthalate
Di-n-Octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Jndeno (1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamioe
N-Nitrosodi-n-propylamioe
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
www.c:hemtechford com
MainReport·no SUIT rpt
Sample
Result
WI>
WI>
WI>
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
IS
Page 29 of90
Certificate of Analysis
Minimum
Reporting
Limit
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ugiL
ugiL
ugiL
ug/L
ug!L
ug!L
ugiL
ugiL
ug!L
ugiL
ugiL
ugiL
ug!L
ugiL
ugiL
ugiL
ugiL
Analytlul
Method
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page 25 of 37
Lab Sample No.: 1408830.(16
Sample Date: 8/19/2014 10:10 AM
Receipt Date: 8/21/2014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Dateffime
08/2112014· 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
0812212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
0812212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08122/2014 07:52
08/2212014 07:52
08/2212014 07:52
Analysis
Dateffime
812812014 ._2;48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/2812014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
812812014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
8/2812014 2:48
8/2812014 2:48
8/2812014 2:48
8128/2014 2:48
8/28/2014 2:48
8/28/2014 2:48
812812014 2:48
8/28/2014 2:48
8/2812014 2:48
Flag
9632 South 500 West
Sandy, UT 64070
801-262-7299 Olfoce
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell4B
Comments:
Sample Matrix: Water
PO Number:
Parameter
Volatile Organic Compounds
Acetone
Benzene
Carbon Tetrachloride
Chloroform
Chloromethane
Methyl Ethyl Ketone
Methylene Chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, total
www.chemtechford com
MainReport-no surr rpl
Sample
Result
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
Page 30 of90
Certificate of Analysis
Minimum
Reporting
Limit
700
5.0
5.0
70.0
30.0
4000
5.0
100
46.0
1000
10000
Units
uglL
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug/L
ug!L
Analytical
Method
EPA S260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
Page26 of 37
Lab Sample No.: 1408830-06
Sample Date: 8/19/2014 10:10 AM
RecelptDate: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill-Groundwater
Preparation
Datetrlme
08/28/2014 19:52
08/28/2014 19:52
08/28/2014 19:52
08/28/2014 19:52
08/28/2014 19:52
08/28/2014 19:52
08/28/2014 19:52
08/28/2014 19:52
08/28/2014 19:52
08/28/2014 19:52
08/28/2014 19:52
Analysis
Date/Time
812812014 19:5'2
8/28/2014 19:52
8/28/2014 19:52
8/28/2014 19:52
8/28/2014 19:52
8/28/2014 19:52
8/28/2014 19:52
8/28/2014 19:52
8/28/2014 19:52
8/28/2014 19:52
8/28/2014 19:52
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: October 14, 2014
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Cell4B
358469006
Ground Water
19-AUG-14 10:10
25-AUG-14
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Total Alpha Radium, Liquid "As Received"
Gross Radium Alpha 1.48E+05 +/-446
MDC
16.6
RL
1.00
Project:
Client ID:
DNMIOOlOO
DNMI001
Units DF Analyst Date Time Batch Method
pCi/L CXP3 10113/14 1537 1426429
The following Analytical Methods were performed: ----------~----------------------------------------------------------------------Method Description ____________ ..:..An=aool. '-"s'-=-t C.omment"-s ---------------------
EPA 900.1 Modified
Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits
Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 104 (25%-125%)
Notes:
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is
the greater of either the adjusted MDL or the CRDL.
Page 17 of21
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 4B LDS
Comments:
Sample Matrix: Water
PO Number:
Parameter
Calculations
Auiom. lomt
Cation!Aoion Balance
Cations, Total
TDS Balance
Inorganic
AlfcalTnily -Bicarbonate (HC03)
Alkalinity -Carbonate ( C03)
AmmoniaasN
Chloride
Conductivity
Fluoride
Nitrate +Nitrite, Total
pH
Sulfate
Total Dissolved Solids (TDS)
TDS, Calculated
Vletals
Arsenic, Dissolved
Beryllium, Dissolved
Calcium, Dissolved
Cadmium, Dissolved
Cobalt, Dissolved
Chromium, Dissolved
Copper, Dissolved
Iron, Dissolved
Lead, Dissolved
Mercury, Dissolved
Magnesium, Dissolved
Manganese, Dissolved
Molybdenum, Dissolved
Nickel, Dissolved
Potassium, Dissolved
Selenium, Dissolved
Silver, Dissolved
Tin, Dissolved
Sodium, Dissolved
www.chemtechford.com
Main Report-no surr rpl
Sample
Result
1910
-43
760
80
ND
ND
5240
6900
76300
970
43.0
2.2
82300
129000
103000
67.8
0.282
308
2.29
23.3
6.16
308
2590
4.12
0.0020
3400
144
24.3
40.1
952
4.08
0.119
ND
6920
Page 31 of 90
Certificate of Analysis
Minimum
Reporting
Limit
1.0
1.0
25.0
100
50.0
10.0
0.1
1000
1000
5
5.00
0.010
2.0
2.00
5.00
5.00
10.0
11.0
0.0500
0.0020
2.0
0.800
5.00
5.00
5.0
0.0500
0.100
17.0
5.0
Units
meq/t
%
meq/L
%
nWl-
mg/L
mg/L
mg!L
umbo/em
mg/L
mg/L
pH Units
mg!L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Lab Sample No.: 1408830..07
Sample Date: 8/19/2014 10:00 AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Analytical
Method
SM t030E
SM 1030E
SM 1030E
SM2340B
SM'2310B
SM2320B
SM 4500 NH3-D
EPA300.0
EPA 120.1
EPA300.0
EPA353.2
SM4500H-B
EPA300.0
SM2540C
SM2540C
EPA200.8
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA245.1
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.7
Preparation
Daterrlme
09/12/2014 12:47
09/12/2014 12:47
09/12/2014 12:47
09/12/2014 12:47
09/02/2014 00:00
09/02/2014 00:00
09/01/2014 19:00
08/29/2014 17:00
08/22/20 14 13 :20
08/29/2014 17:00
09/04/2014 14:15
08/21/2014 08:18
08/29/2014 17:00
08/21/2014 13:32
09/12/2014 12:47
08128/2014 10:16
08125/2014 13:13
08/25/2014 13:13
08/28/2014 10:16
08/28/2014 10:16
08/28/2014 10:16
08/28/2014 10:16
08/25/20 14 13: 13
08129/2014 11:05
09/05/2014 16:11
08/25/2014 l3: 13
08/25/2014 13:13
08/2812014 10:16
08128/2014 10:16
08/25/2014 13:13
08/29/2014 11:05
08/29/2014 11:05
08/25/2014 13:13
08125/2014 13:13
Analysu
Daterrime
9/12/2014 13:05
9/12/2014 13:05
9/12/2014 13:05
9/12/2014 14:28
9/2/2014 16:01
9/2/2014 16:01
9/1/2014 19:00
8/29/2014 17:00
8/22/2014 13:25
8/29/2014 17:00
9/4/2014 14:15
8/21/2014 8:18
8/29/2014 17:00
8/21/2014 13:32
9/12/2014 14:28
8/28/2014 15:30
8/25/2014 16:47
8/25/2014 16:47
8/28/2014 15:30
8/28/2014 15:30
8/28/2014 15:30
8/28/2014 15:30
8/25/2014 16:47
8/29/2014 13:35
9/8/2014 8:45
8/25/2014 16:47
8/25/2014 16:47
8/28/2014 15:30
8/28/2014 15:30
8/25/2014 16:47
8/29/2014 13:35
8/29/2014 13:35
8/25/2014 16:47
8/25/2014 16:47
Flag
SPH
Page 27of37 9632 South 500 West
Sandy. UT 84070
601-262-7299 OffiCe
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell4B LDS
Comments:
Sample Matrix: Water
PO Number:
Parameter
Metals
111nllium, Dissolved
Vanadium, Dissolved
Zinc, Dissolved
Radiochemistry
I:Jmnium, Oii\6Qivcd
Semi-Volatile Compounds
1-Methylnaphthalene
1,2,4-Trichlorohenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dich1orobenzene
2,4,5-Tricblorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dirnethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3 & 4-Methylphenol
3,3 · -Dicblorobenzidine
4-Chlorophenol
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-melhylphenol
4-Chlorophenyl Phenyl Ether
4-Nitropbenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzidine
wtiW chemtechford com
Main Report-no surr rpt
Sample
Result
0.336
671
144
143
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 32 of90
Certificate of Analysis
Minimum
Reportine
Limit
0.0200
5.00
5.00
5.00
10
10
10
lO
10
10
10
10
lO
20
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Uniu
mg!L
mg!L
mg!L
mg!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ugiL
ug/L
ug!L
ugiL
ug!L
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ug/L
Analytical
Method
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA82700
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA82700
EPA8270D
EPA8270D
EPA8270D
EPA82700
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page 28 o1' 37
Lab Sample No.: 1408830-07
Sample Date: 8/19/2014 10:00 AM
Receipt Date: 8/21/2014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Date/Time
08!2912014 11:05
08/28/2014 10:16
08/25/2014 13:13
08/2812014 lO!l(i
08122/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
Analysis
Date/Time
8/29/2014 13:35
8/28/2014 15:30
8/25/2014 16:47
8/28/2014 15:30
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
Flag
9632 South 500 West
Sandy, UT 64070
801-262-7299 Office
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 4B LOS
Comments:
Sample Matrix: Water
PO Number:
Parameter
Semi-Volatile Compounds
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g,h,i) pery1ene
Benzo (k) fluoranthene
Bis (2~hloroethoxy) Methane
Bis (2~h1oroethy1) Ether
Bis (2~hloroisopropyl) Ether
Bis (2·ethylhexy1) Phthalate
Butylbenzy1phthalate
Chrysene
Dibenzo ( a,h) anthracene
Diethylphthalate
Dimethyl phthalate
Di-n-butylphthalate
Di-n-Octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno (I ,2,3~) pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylarnine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
WWN chemtechford com
MainReport-110 surr.rpl
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
27
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 33 of90
Certificate of Analysis
Minimum
Reporting
Limit
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units
ug/L
ug!L
ug!L
ug/L
ug/L
ug!L
ug!L
ug!L
ug!L
ug/L
ugiL
ug!L
ugiL
ug!L
ug/L
ug!L
ug!L
ug!L
ug!L
ug!L
ugiL
ugiL
ugiL
ug!L
ug!L
ugiL
ug!L
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ug!L
Analytical
Method
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page29 of 37
Lab Sample No.: 1408830..07
Sample Date: 8/19/2014 10:00 AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Dateffime
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
0812212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
0812212014 07:52
08/2212014 07:52
08/2212014 07:52
Analysis
Dateffime
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
8/28/2014 3:14
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 4B LDS
Comments:
Sample Matrix: Water
PO Number:
Parameter
Volatile Organic Compounds
Acc:IOtl.C
Benzene
Carbon Tetrachloride
Chloroform
Chloromethane
Methyl Ethyl Ketone
Methylene Chloride
Naphthalene
Tetrahydrofuran
Toluene
Xy1enes, total
WW'N chemtechford com
MainReport-no surr rpt
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
75.6
ND
ND
Page 34 of90
Certificate of Analysis
Minimum
Reporting
Limit
700.
5.0
5.0
70.0
30.0
4000
5.0
100
46.0
1000
10000
Units
ugiL
ug!L
ug!L
ug/L
ug/L
ug!L
ug!L
ugiL
ugiL
ug!L
ug!L
Analytical
Metbod
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
Page 30 of 37
Lab Sample No.: 1408830-07
Sample Date: 8/19/2014 10:00 AM
RecelptDate: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill-Tailings
Project Number: White Mesa Mill-Groundwater
Preparation
Datefflme
08/28/2014 20: I 0
08/28/2014 20:10
08/28/2014 20:10
08/28/2014 20:10
08/28/2014 20:10
08/28/2014 20:10
08/28/2014 20: I 0
08/28/2014 20:10
08/28/2014 20:10
08/28/2014 20: 10
08/28/2014 20: 10
Analysis
Date/Time
812Broll4 20JIO
8/28/2014 20:10
8/28/2014 20:10
8/28/2014 20:10
8/28/2014 20:10
8/28/2014 20:10
8/28/2014 20:10
8/28/2014 20:10
8/28/2014 20:10
8/28/2014 20:10
8/28/2014 20:10
Flag
9632 South 500 West
Sandy. UT 84070
801-262-7299 Offoce
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: October 14, 2014
Company:
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample 10:
Sample 10:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Cell4B LOS
358469007
Ground Water
19-AUG-14 10:00
25-AUG-14
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Total Alpha Radium, Liquid "As Received"
Gross Radium Alpha 1.81E+05 +/-499
The following Analytical Methods were performed:
Method Descri tion
EPA 900.1 Modified
Surrogate/Tracer Recovery Test
MDC
14.7
Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received"
Notes:
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
RL
1.00
Result
Project:
Client 10:
DNMIOOIOO
DNMIOOI
Units OF Analyst Date Time Batch Method
pCi/L CXP3 10/13/14 1537 1426429
An@r~t Comments
Nominal Recovery% Acceptable Limits
96.4 (25%-125%)
SRL =Sample Reporting Limit. For metals analysis only. When the sample is U qualified and NO, the SRL column reports the value which is
the greater of either the adjusted MDL or the CRDL.
Page 18 of21
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 65
Comments:
Sample Matrix: Water
PO Number:
Parameter
Calculations
AniOilS, Tmnl
Cation/Anion Balance
Cations, Total
TDS Balance
Inorganic
Alk.~linhy-Ulcaibonate (HC03)
Alkalinity-Carbonate (C03)
AmmoniaasN
Chloride
Conductivity
Fluoride
Nitrate + Nitrite, Total
pH
Sulfate
Total Dissolved Solids (TDS)
TDS, Calculated
Arst!nie, Dissolved
Berylliwn, Dissolved
Calciwn, Dissolved
Cadrniwn, Dissolved
Cobalt, Dissolved
Cbromiwn, Dissolved
Copper, Dissolved
Iron, Dissolved
Lead, Dissolved
Mercury, Dissolved
Magnesium, Dissolved
Manganese, Dissolved
Molybdenum, Dissolved
Nickel, Dissolved
Potassium, Dissolved
Selenium, Dissolved
Silver, Dissolved
1m, Dissolved
Sodiwn, Dissolved
WNW dlemtechford oom
MainReport.-no surr.rpl
Sample
Result
1520
-39
675
84
ND
ND
2780
5800
72800
1290
42.5
1.7
65300
100000
83700
66.9
0.188
406
1.63
23.4
4.42
491
2280
12.3
ND
2890
115
34.8
48.2
644
2.24
0.222
ND
6380
Page 35 of90
Certificate of Analysis
Minimum
Reporting
Limit
1.0
1.0
25.0
100
50.0
10.0
0.1
1000
1000
5
s.oo
0.010
2.0
0.0200
5.00
0.100
10.0
11.0
5.00
0.0020
2.0
0.800
5.00
5.00
5.0
0.0500
0.100
17.0
5.0
Units
n1cqll..
%
meq!L
%
mg{L
mg!L
mg!L
mg!L
umbo/em
mg!L
mg!L
pH Units
mg!L
mg!L
mg/L
mg/L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mg!L
mgiL
mg!L
mg!L
mgiL
mg!L
mgiL
mgiL
mgiL
mgiL
mg!L
mg!L
Lab Sample No.: 1408830..08
Sample Date: 8/19/2014 9:40AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill-Groundwater
Analytical
Method
SM 1030 E
SM 1030E
SM 1030E
SM2340B
SM2320B
SM2320B
SM 4500 NH3-D
EPA300.0
EPA 120.1
EPA300.0
EPA353.2
SM4500H-B
EPA300.0
SM2540C
SM2540 C
EPA200.8
EPA200.7
EPA200.7
EPA200.8
EPA200.8
EPA200.7
EPA200.8
EPA200.7
EPA200.8
EPA245.1
EPA200.7
EPA200.7
BPA200.8
EPA200.8
EPA200.7
BPA200.8
EPA200.8
EPA200.7
EPA200.7
Preparation
Date/Time
09/12/2014 12:47
09/12/2014 12:47
09/12/2014 12:47
09/12/2014 12:47
09/02/2014 00:00
09/02/2014 00:00
09/01/2014 19:00
08/29/2014 17:00
08/2212014 13:20
08/29/2014 17:00
09/04/2014 14:15
08/21/2014 08:18
08/29/2014 17:00
08/2112014 13:32
09/1212014 12:47
08/28/2014 10:16
08/25/2014 13:13
08/2512014 13:13
08/29/2014 11:05
08/28/2014 10:16
08/25/2014 13:13
08/28/2014 10:16
08/2512014 13:13
08/28/2014 10:16
09/05/2014 16: II
08/25/2014 13:13
08/25/2014 13:13
08/28/2014 10:16
08128/2014 10:16
08/25/2014 13:13
08/29/2014 11:05
08/29/2014 11:05
08/25/2014 13:13
08/25/2014 13:13
Analysis
Date/Time
911212014 13:05
9/12/2014 13:05
9/12/2014 13:05
9/12/2014 14:28
9(212014 16:01
9/212014 16:01
9/1/2014 19:00
8/29/2014 17:00
8/2212014 13 :25
8/29/2014 17:00
9/4/2014 14:15
8/21/2014 8:18
8/29/2014 17:00
8/2112014 13:32
9/1212014 14:28
8128120)4 15:33
8/25/2014 16:51
8/25/2014 16:51
8/29/2014 13:39
8/28/2014 15:33
8/25/2014 16:51
8/28/2014 15:33
8/25/2014 16:51
8/28/2014 15:33
9/8/2014 8:45
8/25/2014 16:51
8/25/2014 16:51
8/28/2014 15:33
8/28/2014 15:33
8/25/2014 16:51
8/29/2014 13:39
8/29/2014 13:39
8/25/2014 16:51
8/25/2014 16:51
Flag
SPH
Page 31 of 37 9632 Soutl1 500 West
Sandy, UT 84070
801-262-7299 OffiCe
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 65
Comments:
Sample Matrix: Water
PO Number:
Parameter
Metals
'I'Jta.llium, Dissolved
Vanadium, Dissolved
Zinc, Dissolved
Radiochemistry
Urnnlum, Oissolv.:d
Semi-Volatile Compounds
1-M.cthylnaphthnlanc
1,2,4-Trichlorobenzene
I ,2-Dichlorobenzene
I ,3-Dichlorobenzene
1,4-Dichlorobenzene
2,4,5-Trichloropbenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
3 & 4-Methylphenol
3,3 '-Dichlorobenzidine
4-Chlorophenol
4,6-Dinitro-2-melhylphenol
4-Bromophenyl phenyl ether
4-Chlor()-3-methylphenol
4-Chlorophenyl Phenyl Ether
4-Nitropheno1
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzidine
www dlemtechrord.c:om
MainReport-no SUIT rpl
Sample
Result
0.377
491
137
124
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 36 of90
Certificate of Analysis
Minimum
Reporting
Limit
0.0200
5.00
5.00
5.00
10
10
10
10
10
10
10
10
10
20
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units
mgfL
mgfL
mgfL
mg/L
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ugfL
ug!L
ug!L
ugfL
ugfL
ugfL
ugfL
ugfL
Analyti£al
Method
EPA200.8
EPA200.8
EPA200.7
l!PA200.8
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page 32 of 37
Lab Sample No.: 1408830..()8
Sample Date: 8/19/2014 9:40AM
Receipt Date: 8/21/2014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill-Tailings
Project Number: White Mesa Mill-Groundwater
Preparation
Dateffime
0812912014 II :OS
08/28/2014 10:16
08/25/2014 13:13
08/28/2014 10:16
08n212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
Analysis
Dateffime
8/2912014 13:39
8/28/2014 15:33
8/25/2014 16:51
8128/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/2812014 3:40
8/2812014 3:40
812812014 3:40
812812014 3:40
8/2812014 3:40
8128/2014 3:40
812812014 3:40
812812014 3:40
812812014 3:40
812812014 3:40
8/2812014 3:40
812812014 3:40
812812014 3:40
812812014 3:40
812812014 3:40
812812014 3:40
8/2812014 3:40
812812014 3:40
812812014 3:40
8/2812014 3:40
812812014 3:40
812812014 3:40
812812014 3:40
812812014 3:40
812812014 3:40
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 Offoce
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 65
Comments:
Sample Matrix: Water
PO Number:
Parameter
Semi-Volatile Compnunds
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g,h,i) perylene
Benzo (k) fluoranthene
Bis (2-chloroethoxy) Methane
Bis (2-chloroethy1) Ether
Bis (2-chloroisopropyl) Ether
Bis (2-ethylhexyl) Phthalate
Butylbenzy !phthalate
Chrysene
Dibenzo (a,h) anthracene
Diethylphthalate
Dimethyl phthalate
Di-n-butylphthalate
Di-n-Octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexacblorobutadiene
Hexacblorocyclopentadiene
Hexachloroethane
Indeno (1,2,3-cd) pyrene
lsopborone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
www.chemlechford com
Main Report-no surr rpt
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 37 of90
Certificate of Analysis
Minimum
Reporting
Limit
1.0
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
lO
10
lO
10
10
10
10
lO
10
lO
10
10
10
lO
lO
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
ugiL
Analytical
Method
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
EPA8270D
Page 33 of 37
Lab Sample No.: 1408830.08
Sample Date: 8/19/2014 9:40AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Datefflme
08/22/2014 ()7:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08122/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/22/2014 07:52
08/2212014 07:52
08/2212014 07:52
Analysis
Daterrlme
81'28/2014 :MO
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
8/28/2014 3:40
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Cell 65
Comments:
Sample Matrix: Water
PO Number:
Parameter
Volatile Organic Compounds
Acetone
Benzene
Carbon Tetrachloride
Chloroform
Chloromethane
Methyl Ethyl Ketone
Methylene Chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, total
w.rw chemtechford com
MainReport-no SUIT rpt
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 38 of90
Certificate of Analysis
Minimum
Reporting
Limit
700
5.0
5.0
70.0
30.0
4000
5.0
!00
46.0
!000
!0000
Units
u&IL
ug/L
ug/L
ug!L
ug!L
ug/L
ug!L
ug!L
ug/L
ug!L
ug!L
Analytical
Metbod
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
Page 34of37
Lab Sample No.: 1408830..()8
Sample Date: 8/19/2014 9:40AM
Receipt Date: 8/2112014 8:30AM
Sampler: Garrin Palmer
Project: White Mesa Mill -Tailings
Project Number: White Mesa Mill -Groundwater
Preparadon
Date/Time
0812812014 20:28
08/28/2014 20:28
08/28/2014 20:28
08/28/2014 20:28
08/28/2014 20:28
08/28/2014 20:28
08/28/2014 20:28
08/28/2014 20:28
08/28/2014 20:28
08/28/2014 20:28
08/28/2014 20:28
Analysis
Daterrlme
8/28/2014 20:28
8/28/2014 20:28
8/28/2014 20:28
8/28/2014 20:28
8/28/2014 20:28
8/28/2014 20:28
8/28/2014 20:28
8/28/2014 20:28
8/28/2014 20:28
8/28/2014 20:28
8/28/2014 20:28
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 OffiCe
CHEMTECH-FORD
LABORATORIES
Name: Energy Fuels
Sample Site: Trip Blank
Comments:
Sample Matrix: Water
PO Number:
Parameter
Volatile Organic ComJwunds
Acetone
Benzene
Carbon Tetrachloride
Chloroform
Chloromethane
Methyl Ethyl Ketone
Methylene Chloride
Naphthalene
Tetrahydrofuran
Toluene
Xylenes, total
www chemtechford com
MainReport--no surr.rpt
Sample
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page 39 of90
Certificate of Analysis
Minimum
Reporting
Limit
700
5.0
5.0
70.0
30.0
4000
5.0
100
46.0
1000
10000
Unita
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
ug!L
Analytleal
Method
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
EPA8260B
Page 35 of 37
Lab Sample No.: 1408830..(19
Sample Date: 8/19/2014 12:00 AM
RecelptDate: 8/21/2014 8:30AM
Sampler:
Project: White Mesa Mill-Tailings
Project Number: White Mesa Mill -Groundwater
Preparation
Date/Time
·0'8127/2014 14:08
08/27/2014 14:08
08/27/2014 14:08
08/27/2014 14:08
08/27/2014 14:08
08/27/2014 14:08
08/27/2014 14:08
08/27/2014 14:08
08/27/2014 14:08
08/27/2014 14:08
08/27/2014 14:08
Analysis
Date/Time
8/27/2014 14:08
8/27/2014 14:08
8/27/2014 14:08
8/27/2014 14:08
8/27/2014 14:08
8/27/2014 14:08
8/27/2014 14:08
8/27/2014 14:08
8/27/2014 14:08
8/27/2014 14:08
8/27/2014 14:08
Flag
9632 South 500 West
Sandy, UT 84070
801-262-7299 OffiCe
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: October 14, 2014
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
White Mesa Mill GW
Cell65
358469008
Ground Water
19-AUG-14 09:40
25-AUG-14
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Total Alpha Radium, Liquid "As Received"
Gross Radium Alpha 1.66E+05 +/-421
The following Analytical Methods were performed:
Method
Surrogate/Tracer Recovery"--_T_e_st_
MDC
11.5
Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received"
Notes:
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
RL
1.00
Result
Project:
Client ID:
DNMIOOlOO
DNMIOOl
Units DF Analyst Date Time Batch Method
pCi/L CXP3 10/14/14 1009 1426429
Nominal Reco~eryo/~ Acceptable Limits
104 (25%-125%)
SRL =Sample Reporting Limit. For metals analysis only. When the sample is U qualified and NO, the SRL column reports the value which is
the greater of either the adjusted MDL or the CRDL.
Page 19 of21
9632 South 500 West
CH EMTECH-FORD
LABORATORIES
10/16/2014
VVorkOrder: 1408830
Energy Fuels
Attn: Garrin Palmer
6425 South Highway 191
Blanding, UT 84511
Client Service Contact: 801.262.7299
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Approved By:
Sandy, Utah 84070 801.262.7299 Main 866.792.0093 Fax
Serving the Intermountain West since 1953
Page 1 of90
www.chemtechfon:l.com
Page 2 of90
Case Narrative for Sample Delivery Group -1408830
CHEMTECH·FORD
Energy Fuels
SampleiD Sam pleNa me Matrix Sampled Received
1408830-01 Cell1 Water 08/19/2014 08/21/2014
1408830-02 Cell2 Slimes Water 08/19/2014 08/21/2014
1408830-03 Cell 3 Water 08/19/2014 08/21/2014
1408830-04 Ceii4A Water 08/19/2014 08/21/2014
1408830-05 Ceii4A LOS Water 08/19/2014 08/21/2014
1408830-0SRE Ceii4A LOS Water 08/19/2014 08/21/2014
1408830-06 Ceii4B Water 08/19/2014 08/21/2014
1408830-07 Ceii4B LOS Water 08/19/2014 08/21/2014
1408830-08 Cell65 Water 08/19/2014 08/21/2014
1408830-09 Trip Blank Water 08/19/2014 08/21/2014
Method Blanks
All method blanks were below the Minimum Reporting Limit (MRL) except for those mentioned in the QC report.
Laboratory Control Samples
All Laboratory Control Sample (LCS) recoveries were within laboratory control limits.
Holding Times
All preparations and analyses were performed within holding times
Matrix Spike/Matrix Spike Duplicate
All Matrix Spike/Matrix Spike Duplicate (MS/MSD) recoveries were within control except for those mentioned in the QC
report.
Surrogates
All surrogates were within laboratory control limits.
LabJO:
Client 10:
1408830-01
Cell1
Matrix: Water
Lab ID:
Analyses
EPA 120.1
EPA 200.7
EPA 200.8
EPA 245.1
EPA 300.0
EPA 353.2
EPA 82608
EPA 82700
SM 1030 E
SM 2320 8
SM 2340 8
SM 2540 C
SM 4500 H-8
SM 4500 NH3-D
Client 10:
1408830-02
Cell2 Slimes
Water Matrix:
Lab 10:
Analyses
EPA 120.1
EPA 200.7
EPA 200.8
EPA 245.1
EPA 300.0
EPA 353.2
EPA 82608
EPA 82700
SM 1030 E
SM 2320 B
SM 2340 8
SM 2540C
SM 4500 H-8
SM 4500 NH3-D
Client ID:
1408830-03
Cell3
Water Matrix:
Analyses
EPA 120.1
Page 3 of90
Analytical Summary -1408830
lab 10:
EPA 200.7
EPA 200.8
EPA 245.1
EPA 300.0
EPA 353.2
EPA 8260B
EPA 82700
SM 1030 E
SM 2320 8
SM 2340 B
SM 2540 C
SM 4500 H-B
SM 4500 NH3-0
ClientiD:
1408830-04
Ceii4A
Water Matrix:
Lab 10:
Analyses
EPA 120.1
EPA 200.7
EPA 200.8
EPA 245.1
EPA 300.0
EPA 353.2
EPA 8260B
EPA 82700
SM 1030 E
SM 2320 B
SM 2340 B
SM 2540 C
SM 4500 H-B
SM 4500 NH3-0
ClientiD:
1408830-05
Ceii4A LOS
Water Matrix:
Analyses
EPA 120.1
EPA 200.7
EPA 200.8
EPA 245.1
EPA 300.0
EPA 353.2
EPA 82608
EPA 82700
SM 1030 E
Page 4 of90
LabiO:
SM 2320 B
SM 2340 B
SM 2540 C
SM 4500 H-B
SM 4500 NH3-0
ClientiO:
1408830-05RE1
Ceii4A LOS
Water Matrix:
Lab 10:
Analyses
EPA 200.8
ClientiO:
1408830-06
Ceii4B
Matrix: Water
Lab 10:
Analyses
EPA 120.1
EPA 200.7
EPA 200.8
EPA 245.1
EPA 300.0
EPA 353.2
EPA 82608
EPA 82700
SM 1030 E
SM 2320 B
SM 2340 B
SM 2540 C
SM 4500 H-B
SM 4500 NH3-0
Client 10:
1408830-07
Ceii4B LOS
Matrix: Water
Analyses
EPA 120.1
EPA 200.7
EPA 200.8
EPA245.1
EPA 300.0
EPA 353.2
EPA 82608
EPA 82700
SM 1030 E
SM 2320 B
SM 2340 B
Page 5 of90
Lab 10:
SM 2540 C
SM 4500 H-B
SM 4500 NH3-0
Client 10:
1408830-08
Cell65
Matrix: Water
Lab 10:
Analyses
EPA 120.1
EPA 200.7
EPA 200.8
EPA 245.1
EPA 300.0
EPA 353.2
EPA 82608
EPA 82700
SM 1030 E
SM 2320 B
SM 2340 B
SM 2540 C
SM 4500 H-B
SM 4500 NH3-0
Client 10:
1408830-09
Trip Blank
Water Matrix:
Analyses
EPA 82608
Page 6 of90
Page40 of90
QC Summary for Sample Delivery Group -1408830
QCID Analyte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Analyzed MDL MRL OF
Calibration Blank -Method EPA 120.1
4H22009-CCB1 Conductivltv 0.5 4H22009 08/22/14 08/25/14 1
4H22009-CCB2 ConductivitY 0.4 4H22009 08/22/14 08/25/14 1
4H22010-CC81 ConductivitY 0.4 4H22010 08/22/14 08/22/14 l
Calibration Check-Method EPA 120.1
4H22009-CCV1 Conductivity 99.9 90 110 1410 1410 4H22009 08/22/14 08/25/14 1
4H22009-CCV2 Conductivity 99.4 90 110 1400 1410 4H22009 08/22/14 08/25/14 1
4H22010-CCV1 Conductivity 99.8 90 110 1410 1410 4H22010 08/22/14 08/22/14 1
Duplicate-Method EPA 120.1
8408675-DUP1 Conductivity 3.12 20 7980 X\:\XXXX XX 8230 8408675 08/22/14 08/25/14 0.2 1 1
8408675-DUP2 Conductivity 1.49 20 400 >-XXXXXi\-:(X 406 8408675 08/22/14 08/25/14 0.2 1 1
8408676-DUP1 Conductivity 0.093 20 53600 1408830-05 53600 8408676 08/22/14 08/22/14 0.2 1
Initial Cal Blank -Method EPA 120.1
4H22009-ICB1 Conductivity 0.5 4H22009 08/22/14 08/25/14 1
4H22010-ICB1 ConductivitY 0.4 4H22010 08/22/14 08/22/14
Initial Cal Check -Method EPA 120.1
4H22009-ICV1 Conductivity 102 90 110 1430 1410 4H22009 08/22/14 08/25/14 1
4H22010-ICV1 Conductivity 101 90 110 1420 1410 4H22010 08/22/14 08/22/14 l
Page 1 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 41 of90 Ana vzed MDL MRL DF
Blank-Method EPA 200.7
8408729-8LK1 8ervllium, Dissolved -0.000 8408729 08/25/14 08/25/14 0.00 0.00 1
8408729-8LK1 Calcium. Dissolved 0.03 8408729 08/25/14 08/25/14 0.00 0.2 1
8408729-8LK1 Chromium, Dissolved -0.000 8408729 08/25/14 08/25/14 0.00 0.00
8408729-8LK1 Iron, Dissolved 0.001 8408729 08/25/14 08/25/14 0.00 0.02 1
8408729-8LK1 Ma~nesium. Dissolved 0.01 8408729 08/25/14 08/25/14 0.01 0.2 1
8408729-8LK1 Man~anese. Dissolved -0.000 8408729 08/25/14 08/25/14 0.00 0.00 1
8408729-8LK1 Potassium, Dissolved 0.01 8408729 08/25/14 08/25/14 0.04 0.5
8408729-8LK1 Sodium, Dissolved 0.03 8408729 08/25/14 08/25/14 0.02 0.5 .
8408729-8LK1 Tin, Dissolved 0.0008 8408729 08/25/14 08/25/14 0.00 0.02 1
8408729-8LK1 Zinc, Dissolved 0.0001 8408729 08/25/14 08/25/14 0.00 0.01 1
8408730-8LK1 8ervllium, Dissolved 0.0000 8408730 08/25/14 08/25/14 0.00 0.00 1
8408730-8LK1 Calcium. Dissolved 0.01 8408730 08/25/14 08/25/14 0.00 0.2 1
8408730-8LK1 Chromium. Dissolved -0.000 8408730 08/25/14 08/25/14 0.00 0.00 1 -
8408730-8LK1 Iron. Dissolved 0.02 8408730 08/25/14 08/25/14 0.00 0.02 1
QB-01-The method blank contains analyte at a concentration above the MRL; however, concentration is less than 10% ofthe sample result, which is negligible according to method criteria.
8408730-8LK1 Ma~nesium, Dissolved 0.03 8408730 08/25/14 08/25/14 0.01 0.2 1
8408730-8LK1 Man~anese. Dissolved 0.002 8408730 08/25/14 08/25/14 0.00 0.00 1
8408730-8LK1 Potassium, Dissolved 0.02 8408730 08/25/14 08/25/14 0.04 0.5 1
8408730-8LK1 Sodium. Dissolved 0.1 8408730 08/25/14 08/25/14 0.02 0.5 1
B408730-8LK1 Tin. Dissolved 0.002 8408730 08/25/14 08/25/14 0.00 0.02 1
8408730-8LK1 Zinc. Dissolved 0.004 8408730 08/25/14 08/25/14 0.00 0.01 1
Calibration Blank-Method EPA 200.7
4H25014-CC81 Bervllium, Dissolved 0.0002 4H25014 08/25/14 08/25/14 1
4H25014-CCB1 Calcium, Dissolved 0.004 4H25014 08/25/14 08/25/14 -
4H25014-CCB1 Chromium, Dissolved 0.0002 4H25014 08/25/14 08/25/14 1
4H25014-CCB1 Iron. Dissolved 0.0005 4H25014 08/25/14 08/25/14 1
Page 2 of43
QCID Analvte %Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 42 of90 Ana vzed MDL MRL DF
4H25014-CCB1 MaRnesium, Dissolved 0.01 4H25014 08/25/14 08/25/14
4H25014-CCB1 ManRanese, Dissolved 0.0003 4H25014 08/25/14 08/25/14
4H25014-CCB1 Potassium, Dissolved 0.01 4H25014 08/25/14 08/25/14 1
4H25014-CCB1 Sodium, Dissolved 0.01 4H25014 08/25/14 08/25/14 1
4H25014-CCB1 Tin, Dissolved 0.003 4H25014 08/25/14 08/25/14
4H25014-CCB1 Zinc, Dissolved 0.0005 4H25014 08/25/14 08/25/14 1
4H25014-CCB2 Bervllium, Dissolved 0.0002 4H25014 08/25/14 08/25/14 1 -
4H25014-CCB2 Calcium, Dissolved 0.02 4H25014 08/25/14 08/25/14
4H25014-CCB2 Chromium, Dissolved 0.0003 4H25014 08/25/14 08/25/14
4H25014-CCB2 Iron, Dissolved 0.02 4H25014 08/25/14 08/25/14 1
4H25014-CCB2 MaRnesium, Dissolved 0.03 4H25014 08/25/14 08/25/14 1
4H25014-CCB2 ManRanese, Dissolved 0.002 4H25014 08/25/14 08/25/14 1
4H25014-CCB2 Potassium, Dissolved 0.03 4H25014 08/25/14 08/25/14
4H25014-CCB2 Sodium, Dissolved 0.1 4H25014 08/25/14 08/25/14 1
4H25014-CCB2 Tin, Dissolved 0.004 4H25014 08/25/14 08/25/14 1
4H25014-CCB2 Zinc, Dissolved 0.008 4H25014 08/25/14 08/25/14
4H25014-CCB3 Bervllium, Dissolved 0.0003 4H25014 08/25/14 08/25/14 1
4H25014-CCB3 Calcium. Dissolved 0.008 4H25014 08/25/14 08/25/14 1
4H25014-CCB3 Chromium, Dissolved 0.0001 4H25014 08/25/14 08/25/14 1
4H25014·CCB3 Iron, Dissolved 0.01 4H25014 08/25/14 08/25/14 1
4H25014-CCB3 Ma~nesium. Dissolved 0.02 4H25014 08/25/14 08/25/14 1
4H25014-CCB3 Man~anese, Dissolved 0.003 4H25014 08/25/14 08/25/14 1
4H25014·CCB3 Potassium, Dissolved 0.03 4H25014 08/25/14 08/25/14 1
4H25014·CCB3 Sodium, Dissolved 0.2 4H25014 08/25/14 08/25/14 1 -
4H25014-CCB3 Tin, Dissolved 0.003 4H25014 08/25/14 08/25/14
4H25014-CCB3 Zinc, Dissolved 0.004 4H25014 08/25/14 08/25/14 1
Page 3 of43
QCID Analvte
4H25014-CCV1 Bervllium. Dissolved
4H25014-CCV1 Calcium. Dissolved
4H25014-CCV1 Chromium, Dissolved
4H25014-CCV1 Iron. Dissolved
4H25014-CCV1 MaRnesium. Dissolved
4H25014·CCV1 ManRanese. Dissolved
4H25014·CCV1 Potassium. Dissolved
4H25014-CCV1 Sodium. Dissolved
4H25014·CCV1 Tin. Dissolved
4H25014-CCV1 Zinc, Dissolved
4H25014-CCV2 Bervllium, Dissolved
4H25014-CCV2 Calcium, Dissolved
4H25014·CCV2 Chromium. Dissolved
4H25014-CCV2 Iron. Dissolved
4H25014-CCV2 Ma~nesium. Dissolved
4H25014·CCV2 Man~anese. Dissolved
4H25014-CCV2 Potassium. Dissolved
4H25014-CCV2 Sodium. Dissolved
4H25014-CCV2 Tin. Dissolved
4H25014-CCV2 Zinc. Dissolved
4H25014-CCV3 Bervllium. Dissolved
4H25014-CCV3 Calcium, Dissolved
4H25014-CCV3 Chromium. Dissolved
4H25014-CCV3 Iron. Dissolved
4H25014-CCV3 Ma~~:nesium, Dissolved
Page 4 of 43
% Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch
Calibration Check-Method EPA 200.7
101 90 110 2.03 2.00 4H25014
100 90 110 2.0 2.00 4H25014
97.6 90 110 1.95 2.00 4H25014
104 90 110 2.08 2.00 4H25014
99.4 90 110 2.0 2.00 4H25014
97.8 90 110 1.96 2.00 4H25014
99.7 90 110 19.9 20.0 4H25014
97.5 90 110 19.5 20.0 4H25014
99.9 90 110 2.00 2.00 4H25014
102 90 110 2.04 2.00 4H25014
101 90 110 2.01 2.00 4H25014
92.5 90 110 1.9 2.00 4H25014
98.1 90 110 1.96 2.00 4H25014
102 90 110 2.04 2.00 4H25014
99.6 90 110 2.0 2.00 4H25014
98.4 90 110 1.97 2.00 4H25014
99.2 90 110 19.8 20.0 4H25014
98.2 90 110 19.6 20.0 4H25014
100 90 110 2.01 2.00 4H25014
100 90 110 2.01 2.00 4H25014
101 90 110 2.01 2.00 4H25014
99.3 90 110 2.0 2.00 4H25014
97.7 90 110 1.95 2.00 4H25014
104 90 110 2.08 2.00 4H25014
100 90 110 2.0 2.00 4H25014
Sampled Prepared Paae 43 of90 Analvzed MDL MRL OF
08/25/14 08/25/14
08/25/14 08/25/14 1
08/25/14 08/25/14
08/25/14 08/25/14 1
08/25/14 08/25/14
08/25/14 08/25/14 l
08/25/14 08/25/14 l
08/25/14 08/25/14 1
08/25/14 08/25/14 [
08/25/14 08/25/14 I
08/25/14 08/25/14 1
08/25/14 08/25/14 1
08/25/14 08/25/14
08/25/14 08/25/14 1
08/25/14 08/25/14 1
08/25/14 08/25/14 1
08/25/14 08/25/14
08/25/14 08/25/14 1
08/25/14 08/25/14 1
08/25/14 08/25/14 1
08/25/14 08/25/14 1
08/25/14 08/25/14 1
08/25/14 08/25/14 1
08/25/14 08/25/14 1
08/25/14 08/25/14 l
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 44 of90 Ana vzed MDL MRL OF
4H25014-CCV3 Man~~:anese. Dissolved 98.1 90 110 1.96 2.00 4H25014 08/25/14 08/25/14 1
4H25014·CCV3 Potassium, Dissolved 100 90 110 20.0 20.0 4H25014 08/25/14 08/25/14
4H25014-CCV3 Sodium, Dissolved 98.0 90 110 19.6 20.0 4H25014 08/25/14 08/25/14
4H25014·CCV3 Tin. Dissolved 99.0 90 110 1.98 2.00 4H25014 08/25/14 08/25/14 1
4H25014·CCV3 Zinc. Dissolved 103 90 110 2.05 2.00 4H25014 08/25/14 08/25/14 1
Initial Cal Blank -Method EPA 200.7
4H25014·1CB1 Bervllium. Dissolved 0.0002 4H25014 08/25/14 08/25/14
4H25014·1CB1 Calcium, Dissolved 0.01 4H25014 08/25/14 08/25/14 1
4H25014-ICB1 Chromium, Dissolved 0.0002 4H25014 08/25/14 08/25/14 1
4H25014-ICB1 Iron, Dissolved 0.004 4H25014 08/25/14 08/25/14 1
4H25014·1CB1 Ma~~:nesium, Dissolved 0.005 4H25014 08/25/14 08/25/14 1
4H25014-ICB1 Man~~:anese, Dissolved 0.0002 4H25014 08/25/14 08/25/14 1
4H25014-ICB1 Potassium. Dissolved 0.01 4H25014 08/25/14 08/25/14 1
4H25014-ICB1 Sodium. Dissolved 0.002 4H25014 08/25/14 08/25/14 1
4H25014-ICB1 Tin, Dissolved 0.004 4H25014 08/25/14 08/25/14 1
4H25014-ICB1 Zinc. Dissolved 0.0002 4H25014 08/25/14 08/25/14 1
Initial Cal Check -Method EPA 200.7
4H25014-ICV1 Bervllium. Dissolved 99.8 95 105 2.00 2.00 4H25014 08/25/14 08/25/14 1
4H25014-ICV1 Calcium, Dissolved 101 95 105 2.0 2.00 4H25014 08/25/14 08/25/14 1
4H25014-ICV1 Chromium, Dissolved 97.1 95 105 1.94 2.00 4H25014 08/25/14 08/25/14 1
4H25014-ICV1 Iron. Dissolved 102 95 105 2.05 2.00 4H25014 08/25/14 08/25/14
4H25014·1CV1 Ma~~:nesium. Dissolved 97.1 95 105 1.9 2.00 4H25014 08/25/14 08/25/14 1
4H25014-ICV1 Man~~:anese, Dissolved 97.8 95 105 1.96 2.00 4H25014 08/25/14 08/25/14 1
4H25014-ICV1 Potassium, Dissolved 99.7 95 105 19.9 20.0 4H25014 08/25/14 08/25/14
4H25014-ICV1 Sodium. Dissolved 97.4 95 105 19.5 20.0 4H25014 08/25/14 08/25/14 1
4H25014-ICV1 Tin. Dissolved 99.8 95 105 2.00 2.00 4H25014 08/25/14 08/25/14 l
Page 5 of 43
QCID Analvte % Rec RPD
4H25014-ICV1 Zinc. Dissolved 99.3
8408729-851 8ervlllum. Dissolved 97.1
8408729·651 Calcium. Dissolved 91.8
8408729-651 Chromium, Dissolved 98.5
8408729-851 Iron. Dissolved 97.9
6408729-651 Ma11nesium. Dissolved 99.6
8408729·651 Man11anese, Dissolved 99.5
8408729-651 Potassium, Dissolved 93.3
8408729-651 Sodium, Dissolved 96.4
8408729·651 Tin, Dissolved 102
8408729-651 Zinc, Dissolved 94.9
8408730-851 8ervllium, Dissolved 96.7
8408730-8S1 Calcium. Dissolved 91.8
8408730-851 Chromium. Dissolved 97.1
8408730-851 Iron, Dissolved 107
6408730-851 Ma11nesium. Dissolved 95.5
8408730-BS1 Man11anese, Dissolved 98.1
B408730-BS1 Potassium, Dissolved 92.9
6408730-851 Sodium, Dissolved 96.6
8408730-651 Tin, Dissolved 101
8408730-851 Zinc, Dissolved 98.3
6408729-MS1 8ervllium, Dissolved 99.7
8408729-M51 Calcium, Dissolved 110
8408729-MS1 Chromium, Dissolved 101
Page 6 of 43
LCL UCL RPD Max Result QC Source Source Cone Sok Value Surr? Batch
95 105 1.99 2.00 4H25014
LCS-Method EPA 200.7
85 115 0.194 0.200 8408729
85 115 9.4 10.2 8408729
85 115 0.197 0.200 8408729
85 115 0.20 0.200 8408729
85 115 10.2 10.2 8408729
85 115 0.199 0.200 8408729
85 115 7.5 8.00 8408729
85 115 9.6 10.0 8408729
85 155 0.20 0.200 8408729
85 115 0.19 0.200 8408729
85 115 0.193 0.200 8408730
85 115 9.4 10.2 8408730
85 115 0.194 0.200 8408730
85 115 0.21 0.200 8408730
85 115 9.7 10.2 8408730
85 115 0.196 0.200 8408730
85 115 7.4 8.00 8408730
85 115 9.7 10.0 8408730
85 155 0.20 0.200 8408730
85 115 0.20 0.200 8408730
Matrix Spike -Method EPA 200.7
70 130 0.199 XXXXXXX·X\ 0 0.200 8408729
70 130 26.6 XXXXXXX XX 15.4 10.2 8408729
70 130 0.201 XXXXXXX XX 0 0.200 8408729
Sampled Preoared Paae 45 of90 Analvzed MDL MRL OF
08/25/14 08/25/14 l
08/25/14 08/25/14 0.00 0.00
08/25/14 08/25/14 0.00 0.2 1
08/25/14 08/25/14 0.00 0.00 1
08/25/14 08/25/14 0.00 O.D2 1
08/25/14 08/25/14 0.01 0.2 1
08/25/14 08/25/14 0.00 0.00 1
08/25/14 08/25/14 0.04 0.5
08/25/14 08/25/14 0.02 0.5 1
08/25/14 08/25/14 0.00 0.02
08/25/14 08/25/14 0.00 0.01 1
08/25/14 08/25/14 0.00 0.00 1
08/25/14 08/25/14 0.00 0.2 1
08/25/14 08/25/14 0.00 0.00 1
08/25/14 08/25/14 0.00 0.02 1
08/25/14 08/25/14 0.01 0.2 1
08/25/14 08/25/14 0.00 0.00 1
08/25/14 08/25/14 0.04 0.5 1
08/25/14 08/25/14 0.02 0.5
08/25/14 08/25/14 0.00 0.02 1
08/25/14 08/25/14 0.00 0.01 1
08/25/14 08/25/14 0.00 0.00 1
08/25/14 08/25/14 0.00 0.2
08/25/14 08/25/14 0.00 0.00 1
QCID Analvte % Rec RPD LCL UCL
8408729-MS1 Iron, Dissolved 103 70 130
8408729-MS1 MaRnesium, Dissolved 109 70 130
8408729-MS1 ManRanese, Dissolved 101 70 130
8408729-MS1 Potassium, Dissolved 97.7 70 130
8408729-MS1 Sodium. Dissolved 104 70 130
8408729-M$1 Tin. Dissolved 104 70 130
8408729-MS1 Zinc. Dissolved 98 7 70 130
8408729-MS2 Beryllium, Dissolved 100 70 130
RPD Max Result QC Source Source Cone Spk Value Surr? Batch
0.26 :{XX;(;(X\ XX 0.06 0.200 8408729
15.3 XXXXXXX-XX 4,2 10.2 8408729
0.203 ~rxxxxx\ ::~ 0.001 0.200 8408729
8.2 XX)(\\:.{\-);~ 0.4 8.00 8408729
14.2 XX:'\XXXX \X 3.8 10.0 8408729
0.21 Xf::::;(\:< '(.\ 0 0.200 8408729
0.20 X\\X;\X":-XZ 0 0.200 8408729
0.201 XXXXXXi; \X 0 0.200 8408729
Sampled Prepared Page 46 of90 Analyzed MDL MRL OF
08/25/14 08/25/14 0.00 0.02
08/25/14 08/25/14 0.01 0.2
08/25/14 08/25/14 0.00 0.00
08/25/14 08/25/14 0.04 0.5
08/25/14 08/25/14 0.02 0.5
08/25/14 08/25/14 0.00 0.02
08/25/14 08/25/14 0.00 0.01
08/25/14 08/25/14 0.00 0.00 1
B408729-MS2 Calcium, Dissolved -8.03 70 130 445 ~>."<;~><X-XX 446 10.2 8408729 08/25/14 08/25/14 0.00 0.2
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
8408729-M52 Chromium, Dissolved 104 70 130 0.209 -, X\xx;::< ;;:: 0.0001 0.200 8408729 08/25/14 08/25/14 0.00 0.00 1
B408729-MS2 Iron, Dissolved 96.9 70 130 0.28 ';(),o:>:fX ".>' 0.08 0.200 8408729 08/25/14 08/25/14 0.00 0.02
B408729-MS2 Magnesium, Dissolved 99.5 70 130 162 ::-:xx,,.,x-x:, 152 10.2 8408729 08/25/14 08/25/14 0.01 0.2
B408729-MS2 ManRanese, Dissolved 89.2 70 130 0.369 l<XX<X>) X { 0.191 0.200 8408729 08/25/14 08/25/14 0.00 0.00
8408729-MS2 Potassium. Dissolved 96.0 70 130 18.3 \X.C'X{~-XX 10.6 8.00 8408729 08/25/14 08/25/14 0.04 0,5 1
B408729-MS2 Sodium, Dissolved -29.2 70 130 355 ;(7,>:>;\:-:X-\,, 358 10.0 8408729 08/25/14 08/25/14 0.02 0.5 1
QM-4X-The spike recovery was outside of QC acceptance limits for the M5 and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
8408729-M$2 Tin. Dissolved 95.6 70 130 0.20 JX\XX:<:(-):>: 0.008 0.200 8408729 08/25/14 08/25/14 0.00 0.02 1
8408729-MS2 Zinc. Dissolved 93.6 70 130 0.19 >~:,..>~)~XXX-AX 0 0.200 8408729 08/25/14 08/25/14 0.00 0.01 1
B408730-MS1 Bervllium, Dissolved 72.9 70 130 1.64 1408830-05 0.185 2.00 8408730 08/25/14 08/25/14 0.00 0.01 1
8408730-MS1 Calcium, Dissolved 64.2 70 130 402 140883Q-05 336 102 8408730 08/25/14 08/25/14 0.04 2.0 1
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
8408730-MS1 Chromium, Dissolved 69.8 70 130 4.18 1408830-05 2.78 2.00 8408730 08/25/14 08/25/14 0.00 0.05 1
QM-010-The MS recovery was outside acceptance limits but passed Duplicate Spike acceptance limits. The batch was accepted based on the acceptability of the MSD as the batch Spike.
B408730-MS1 Iron, Dissolved 655 70 130 1870 1408830-05 1850 2.00 8408730 08/25/14 08/25/14 0.05 0.20 1
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
8408730-MS1 Magnesium, Dissolved 84.9 70 130 2780 1408830-05 2690 102 8408730 08/25/14 08/25/14 0.1 2.0
8408730-MS1 ManRanese, Dissolved 87.5 70 130 100 1408830-05 98.6 2.00 8408730 08/25/14 08/25/14 0.00 0.05
8408730-M$1 Potassium, Dissolved 71.0 70 130 472 1408830-05 415 80.0 8408730 08/25/14 08/25/14 0.4 5.0
Page 7 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Paqe 47 of90
Ana1vzed MDL MRL DF
8408730-MS1 Sodium. Dissolved 146 70 130 4330 1408830-05 4190 100 8408730 08/25/14 08/25/14 0.2 5.0 1
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
8408730-MS1 Tin. Dissolved 64.9 70 130 1.36 1408830-05 0,06 2.00 8408730 08/25/14 08/25/14 0.02 0.20
QM-RPD -The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the
acceptable recovery of the LCS and the RPD.
6408730-MS1 Zinc. Dissolved -912 70 130 288 1408830-05 306 2.00 8408730 08/25/14 08/25/14 0.01 0.10
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
Matrix Spike Dup -Method EPA 200.7
6408729-MSD1 8ervllium, Dissolved 101 1.41 70 130 20 0.202 X\\\XXX·XX 0 0.200 8408729 08/25/14 08/25/14 0.00 0.00 1
8408729-MSD1 Calcium. Dissolved 109 0.103 70 130 20 26.5 X\XX>.X~-:;;· 15.4 10.2 8408729 08/25/14 08/25/14 0.00 0.2 1
8408729-MSD1 Chromium, Dissolved 102 1.71 70 130 20 0.205 :<:<\XXX:(. :>: 0 0.200 8408729 08/25/14 08/25/14 0.00 0.00 1
8408729-MSD1 I ron, Dissolved 107 2.94 70 130 20 0.27 ~x -:xxx~~-xx o.o6 0.200 8408729 08/25/14 08/25/14 0.00 0.02 1
8408729-MSD1 Magnesium, Dissolved 100 5.82 70 130 20 14,5 x x~v:>:xx-\:< 4.2 10.2 8408729 08/25/14 08/25/14 0.01 0.2 1
8408729-MSD1 Manganese. Dissolved 103 1.77 70 130 20 0.206 xx):.>.xx;~.xx 0.001 0.200 8408729 08/25/14 08/25/14 0.00 0.00
8408729-MSD1 Potassium, Dissolved 99.2 1.44 70 130 20 8.3 XXX\\\>.-),){ 0.4 8.00 8408729 08/25/14 08/25/14 0.04 0.5 1
8408729-MSD1 Sodium, Dissolved 105 0.616 70 130 20 14.3 xx:cXX\-:\,; 3.8 10.0 8408729 08/25/14 08/25/14 0.02 0.5 1
8408729-MSD1 Tin. Dissolved 108 3.42 70 130 20 0.22 .\:x:<xxxx ;:·· o 0.200 8408729 08/25/14 08/25/14 0.00 0.02
8408729-MSD1 Zinc, Dissolved 101 2.20 70 130 20 0.20 :::<::'~<X>> XA 0 0.200 8408729 08/25/14 08/25/14 0.00 0.01
B408729-MSD2 8ervllium. Dissolved 99.8 0.436 70 130 20 0.200 ::xxxx>.~ ~x o 0.200 8408729 08/25/14 08/25/14 0.00 0,00 1
B408729-MSD2 Calcium. Dissolved -97.1 2.06 70 130 20 436 >;xx>":::\)' >~X 446 10.2 8408729 08/25/14 08/25/14 0.00 0.2
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
B408729-MSD2 Chromium. Dissolved 97.2 7.13 70 130 20 0.195 :\!:X\XXX-XX 0.0007 0.200 8408729 08/25/14 08/25/14 0.00 0.00
8408729-MSD2 Iron, Dissolved 93.1 2.78 70 130 20 0.27 xxxx .. :xx XX 0.08 0.200 8408729 08/25/14 08/25/14 0.00 0.02 1
8408729-MSD2 Mai(nesium, Dissolved 62.1 2.38 70 130 20 159 '.X/.:(>:X\· \(X 152 10.2 8408729 08/25/14 08/25/14 0.01 0.2 1
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
8408729-MSD2 Mam!anese. Dissolved 98.2 4.75 70 130 20 0.387 >:'X)(':\X ;; < 0.191 0.200 8408729 08/25/14 08/25/14 0.00 0.00 1
8408729-MSD2 Potassium, Dissolved 94.9 0,490 70 130 20 18.2 XX\ X/XX :\X 10.6 8.00 8408729 08/25/14 08/25/14 0.04 0.5 1
8408729-MSD2 Sodium, Dissolved -63.4 0.967 70 130 20 351 x:(x>:xx::->:> 358 10.0 8408729 08/25/14 08/25/14 0.02 0.5
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
6408729-MSD2 Tin, Dissolved 98.5 2.95 70 130 20 0.20 :<>:-:n,x::-X:\ 0.008 0.200 8408729 08/25/14 08/25/14 0.00 0.02
Page 8 of 43
QCIO Analvte % Rec RPO LCL UCL
B408729-MSD2 Zinc. Dissolved 91.0 2.84 70 130
6408730-MSD1 6ervllium. Dissolved 74.7 2.16 70 130
RPO Max Result QC Source Source Cone Spk Value Surr? Batch
20 0.18 XXXXXXX-XX 0 0.200 8408729
20 1.68 1408830-05 0.185 2.00 6408730
Sampled Prepared Paoe 48 of90 Analyzed MOL MRL OF
08/25/14 08/25/14 0.00 0.01
08/25/14 08/25/14 0.00 0.01 1
B408730-MSD1 Calcium. Dissolved 62.9 0.324 70 130 20 401 1408830-05 336 102 8408730 08/25/14 08/25/14 0.04 2.0 1
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
8408730-MSDl Chromium. Dissolved 70.4 0.275 70 130 20 4.19 1408830-05 2.78 2.00 8408730 08/25/14 08/25/14 0.00 0.05
8408730-MSD1 Iron. Dissolved -292 1.02 70 130 20 1850 1408830-05 1850 2.00 8408730 08/25/14 08/25/14 0.05 0.20 1
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
8408730-MSD1 Ma~nesium. Dissolved 57.2 1.02 70 130 20 2750 1408830-05 2690 102 8408730 08/25/14 08/25/14 0.1 2.0
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
8408730-MSD1 Manganese, Dissolved -19.8 2.16 70 130 20 98.2 1408830-05 98.6 2.00 8408730 08/25/14 08/25/14 0.00 0.05
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
8408730-MSD1 Potassium, Dissolved 68.2 0.475 70 130 20 470 1408830-05 415 80.0 8408730 08/25/14 08/25/14 0.4 5.0 1
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
8408730-MSD1 Sodium, Dissolved 221 1.70 70 130 20 4410 1408830-05 4190 100 8408730 08/25/14 08/25/14 0.2 5.0 1
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
8408730-MSD1 Tin. Dissolved 64.6 0.434 70 130 20 1.35 1408830-05 0.06 2.00 8408730 08/25/14 08/25/14 0.02 0.20 1
QM-RPD-The recovery was outside acceptance limits for the MS and/or MSD. The RPD between the MS and MSD was acceptable and indicates the recovery is due to matrix interference. The batch was accepted based on the
acceptable recovery of the LCS and the RPD.
8408730-MSD1 Zinc. Dissolved 65.5 6.56 70 130 20 308 1408830-05 306 2.00 8408730 08/25/14 08/25/14 0.01 0.10 1
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
Page 9 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cont Spk Value Surr? Batch Samoled Prepared Pa~e 49 of90 Ana vzed MDL MRL OF
Blank -Method EPA 200.8
8408836-BLK1 Arsenic. Dissolved 0.0000 8408836 08/28/14 08/28/14 0.00 0.00 1
B408836-BLK1 Cadmium, Dissolved -0.000 8408836 08/28/14 08/28/14 0.00 0.00 1
B408836-8LK1 Chromium, Dissolved -0.000 8408836 08/28/14 08/28/14 0.00 0.00 1
8408836-8LK1 Cobalt. Dissolved -0.000 8408836 08/28/14 08/28/14 0.00 0.00 1
8408836-8LK1 Coooer. Dissolved -0.000 8408836 08/28/14 08/28/14 0.00 0.00 1 -
8408836-8LK1 lead. Dissolved 0.0000 8408836 08/28/14 08/28/14 0.00 0.00 1
8408836-BLK1 Molybdenum, Dissolved -0.000 8408836 08/28/14 08/28/14 0.00 0.00 1
8408836-BLK1 Nickel, Dissolved 0.0000 8408836 08/28/14 08/28/14 0.00 0.00 1
8408836-8LK1 Selenium, Dissolved 0.0000 8408836 08/28/14 08/28/14 0.00 0.00 1
8408836-BLK1 Silver. Dissolved -0.000 8408836 08/28/14 08/28/14 0.00 0.00 1
8408836-BLK1 Thallium, Dissolved -0.000 8408836 08/28/14 08/28/14 0.00 0.00 1
8408836-8LK1 Uranium, Dissolved -0.000 8408836 08/28/14 08/28/14 0.00 0.00 1
8408836-BLK1 Vanadium. Dissolved 0.0000 8408836 08/28/14 08/28/14 0.00 0.00 1
8408889-8LK1 Arsenic. Dissolved 0.0000 8408889 08/29/14 08/29/14 0.00 0.00
8408889-8LK1 Cadmium. Dissolved -0.000 8408889 08/29/14 08/29/14 0.00 0.00 1
8408889-8LK1 lead. Dissolved 0.0000 8408889 08/29/14 08/29/14 0.00 0.00 1
8408889-8LK1 Molvbdenum. Dissolved 0.0000 8408889 08/29/14 08/29/14 0.00 0.00 1 .
8408889-8LK1 Selenium. Dissolved 0.0000 8408889 08/29/14 08/29/14 0.00 0.00 1 -
8408889-8LK1 Silver. Dissolved 0.0000 8408889 08/29/14 08/29/14 0.00 0.00 1
8408889-8LK1 Thallium, Dissolved 0.0000 8408889 08/29/14 08/29/14 0.00 0.00 1
Calibration Blank -Method EPA 200.8
4H28008-CC8 1 Arsenic, Dissolved 0.0000 4H28008 08/28/14 08/28/14
4H28008-CC81 Cadmium, Dissolved -0.000 4H28008 08/28/14 08/28/14
4H28008-CC81 Chromium. Dissolved 0.0001 4H28008 08/28/14 08/28/14
4H28008-CC81 Cobalt, Dissolved -0.000 4H28008 08/28/14 08/28/14
Page 10 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 50 of90 Ana vzed MDL MRL OF
4H28008-CCB1 Coooer, Dissolved 0.0000 4H28008 08/28/14 08/28/14
4H28008-CCB1 Lead. Dissolved -0.000 4H28008 08/28/14 08/28/14 l
4H28008-CCB1 Molvbdenum. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-CCB1 Nickel. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-CCB1 Selenium. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-CCB1 Silver. Dissolved -0.000 4H28008 08/28/14 08/28/14
4H28008-CCB1 Thallium. Dissolved 0.0000 4H28008 08/28/14 08/28/14
4H28008-CCB1 Uranium, Dissolved -0.000 4H28008 08/28/14 08/28/14
4H28008-CCB1 Vanadium, Dissolved 0.0000 4H28008 08/28/14 08/28/14
4H28008-CCB2 Arsenic, Dissolved 0.0000 4H28008 08/28/14 08/28/14 1
4H28008-CCB2 Cadmium, Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-CCB2 Chromium, Dissolved 0.0000 4H28008 08/28/14 08/28/14 1
4H28008-CCB2 Cobalt. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-CCB2 Coooer. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-CCB2 Lead. Dissolved -0.000 4H28008 08/28/14 08/28/14
4H28008-CCB2 Molvbdenum. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-CCB2 Nickel. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-CCB2 Selenium. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-CCB2 Silver. Dissolved 0.0000 4H28008 08/28/14 08/28/14
4H28008-CCB2 Thallium, Dissolved 0.0000 4H28008 08/28/14 08/28/14 1
4H28008-CCB2 Uranium. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-CCB2 Vanadium. Dissolved 0.0000 4H28008 08/28/14 08/28/14
4H29006-CCB1 Arsenic, Dissolved 0.0000 4H29006 08/29/14 08/29/14
4H29006-CCB1 Cadmium, Dissolved 0.0000 4H29006 08/29/14 08/29/14
4H29006-CCB1 Lead, Dissolved 0.0000 4H29006 08/29/14 08/29/14 L
4H29006-CCB 1 Molybdenum, Dissolved 0.0002 4H29006 08/29/14 08/29/14 1
Page 11 of 43
QCIO Analvte % Rec RPO LCL UCL RPO Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 51 of90 Ana vzed MDL MRL OF
4H29006-CCB1 Selenium, Dissolved 0.0001 4H29006 08/29/14 08/29/14 l
4H29006-CCB1 Silver, Dissolved 0.0003 4H29006 08/29/14 08/29/14
4H29006-CCB1 Thallium, Dissolved 0.0000 4H29006 08/29/14 08/29/14
4H29006-CCB2 Arsenic, Dissolved 0.0000 4H29006 08/29/14 08/29/14 1
4H29006-CCB2 Cadmium, Dissolved 0.0000 4H29006 08/29/14 08/29/14 1
4H29006-CCB2 Lead, Dissolved 0.0000 4H29006 08/29/14 08/29/14 1
4H29006-CCB2 Molybdenum, Dissolved 0.0003 4H29006 08/29/14 08/29/14 1
4H29006-CCB2 Selenium, Dissolved 0.0000 4H29006 08/29/14 08/29/14
4H29006-CCB2 Silver, Dissolved 0.0002 4H29006 08/29/14 08/29/14 1
4H29006-CCB2 Thallium, Dissolved 0.0000 4H29006 08/29/14 08/29/14 1
4H29006-CCB3 Arsenic, Dissolved 0.0002 4H29006 08/29/14 08/29/14 1
4H29006-CCB3 Cadmium, Dissolved 0.0000 4H29006 08/29/14 08/29/14
4H29006-CCB3 Lead, Dissolved -0.000 4H29006 08/29/14 08/29/14 1
4H29006-CCB3 Molvbdenum, Dissolved 0.0005 4H29006 08/29/14 08/29/14 1
QB-01-The method blank contains analyte at a concentration above the MRL; however, concentration is less than 10% of the sample result, which is negligible according to method criteria.
4H29006-CCB3 Selenium, Dissolved 0.0002 4H29006 08/29/14 08/29/14 t
4H29006-CCB3 Silver, Dissolved 0.0003 4H29006 08/29/14 08/29/14 1
4H29006-CCB3 Thallium. Dissolved 0.0000 4H29006 08/29/14 08/29/14
Calibration Check-Method EPA 200.8
4H28008-CCV1 Arsenic, Dissolved 97.5 90 110 0.039 0.0400 4H28008 08/28/14 08/28/14 l.
4H28008-CCV1 Cadmium. Dissolved 96.9 90 110 0.039 0.0400 4H28008 08/28/14 08/28/14 1
4H28008-CCV1 Chromium, Dissolved 97.8 90 110 0.039 0.0400 4H28008 08/28/14 08/28/14 1
4H28008-CCV1 Cobalt. Dissolved 95.8 90 110 0.038 0.0400 4H28008 08/28/14 08/28/14
4H28008-CCV1 Copper, Dissolved 99.6 90 110 0.040 0.0400 4H28008 08/28/14 08/28/14 1
4H28008-CCV1 Lead, Dissolved 97.6 90 110 0.039 0.0400 4H28008 08/28/14 08/28/14
4H28008-CCV1 Molvbdenum, Dissolved 97.4 90 110 0.039 0.0400 4H2BOOB 08/28/14 08/28/14 1
4H28008-CCV1 Nickel, Dissolved 101 90 110 0.0405 0.0400 4H28008 08/28/14 08/28/14
Page 12 of 43
QCID Analvte % Rec RPD LCL
4H28008-CCV1 Selenium, Dissolved 96.7 90
4H28008-CCV1 Silver, Dissolved 104 90
4H28008-CCV1 Thallium. Dissolved 99.3 90
4H28008-CCV1 Uranium. Dissolved 94.6 90
4H28008-CCV1 Vanadium. Dissolved 103 90
4H28008-CCV2 Arsenic. Dissolved 98.6 90
4H28008-CCV2 Cadmium. Dissolved 94.1 90
4H28008-CCV2 Chromium, Dissolved 99.7 90
4H28008-CCV2 Cobalt, Dissolved 94.4 90
4H28008-CCV2 Copper, Dissolved 97.6 90
4H28008-CCV2 Lead, Dissolved 100 90
4H28008-CCV2 Molvbdenum, Dissolved 96.4 90
4H28008-CCV2 Nickel. Dissolved 101 90
4H28008-CCV2 Selenium, Dissolved 98.1 90
4H28008-CCV2 Silver. Dissolved 101 90
4H28008-CCV2 Thallium. Dissolved 100 90
4H28008-CCV2 Uranium. Dissolved 95.3 90
4H28008-CCV2 Vanadium. Dissolved 105 90
4H29006-CCV1 Arsenic. Dissolved 100 90
4H29006-CCV1 Cadmium, Dissolved 101 90
4H29006-CCV1 Lead. Dissolved 98.4 90
4H29006-CCV1 Molvbdenum, Dissolved 100 90
4H29006-CCV1 Selenium. Dissolved 102 90
4H29006-CCV1 Silver, Dissolved 107 90
4H29006-CCV1 Thallium. Dissolved 99.5 90
4H29006-CCV2 Arsenic, Dissolved 99.6 90
Page 13 of 43
UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch
110 0.039 0.0400 4H28008
110 0.042 0.0400 4H28008
110 0.040 0.0400 4H28008
110 0.038 0.0400 4H28008
110 0.041 0.0400 4H28008
110 0.039 0.0400 4H28008
110 0.038 0.0400 4H28008
110 0.040 0.0400 4H28008
110 0.038 0.0400 4H28008
110 0.039 0.0400 4H28008
110 0,040 0.0400 4H28008
110 0.039 0.0400 4H28008
110 0.0405 0.0400 4H28008
110 0.039 0.0400 4H28008
110 0.040 0.0400 4H28008
110 0.040 0.0400 4H28008
110 0.038 0.0400 4H28008
110 0.042 0.0400 4H28008
110 0.040 0.0400 4H29006
110 0.040 0.0400 4H29006
110 0.039 0.0400 4H29006
110 0.040 0.0400 4H29006
110 0.041 0.0400 4H29006
110 0.043 0.0400 4H29006
110 0.040 0.0400 4H29006
110 0.040 0.0400 4H29006
Sampled Prepared Paae 52 of90 Analyzed MDL MRL OF
08/28/14 08/28/14 1
08/28/14 08/28/14 1
08/28/14 08/28/14 1
08/28/14 08/28/14 .1
08/28/14 08/28/14 1
08/28/14 08/28/14 :!.
08/28/14 08/28/14 1
08/28/14 08/28/14 1
08/28/14 08/28/14 1
08/28/14 08/28/14 1
08/28/14 08/28/14 1
08/28/14 08/28/14 l
08/28/14 08/28/14 1
08/28/14 08/28/14 1
08/28/14 08/28/14 1
08/28/14 08/28/14
08/28/14 08/28/14 1
08/28/14 08/28/14
08/29/14 08/29/14 1
08/29/14 08/29/14 1
08/29/14 08/29/14 1
08/29/14 08/29/14 1
08/29/14 08/29/14 1
08/29/14 08/29/14 1
08/29/14 08/29/14 1
08/29/14 08/29/14 1
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 53 of90 Ana vzed MDL MRL OF
4H29006-CCV2 Cadmium. Dissolved 95.2 90 110 0.038 0.0400 4H29006 08/29/14 08/29/14 1
4H29006-CCV2 Lead. Dissolved 100 90 110 0.040 0.0400 4H29006 08/29/14 08/29/14 1
4H29006-CCV2 Molvbdenum. Dissolved 98.5 90 110 0.039 0.0400 4H29006 08/29/14 08/29/14 1
4H29006-CCV2 Selenium. Dissolved 101 90 110 0.040 0.0400 4H29006 08/29/14 08/29/14
4H29006-CCV2 Silver. Dissolved 107 90 110 0.043 0.0400 4H29006 08/29/14 08/29/14 l
4H29006-CCV2 Thallium. Dissolved 104 90 110 0.042 0.0400 4H29006 08/29/14 08/29/14 1
4H29006-CCV3 Arsenic. Dissolved 102 90 110 0.041 0.0400 4H29006 08/29/14 08/29/14 1
4H29006-CCV3 Cadmium. Dissolved 101 90 110 0.040 0.0400 4H29006 08/29/14 08/29/14 l
4H29006-CCV3 Lead, Dissolved 105 90 110 0.042 0.0400 4H29006 08/29/14 08/29/14 .l
4H29006-CCV3 Molybdenum. Dissolved 106 90 110 0.042 0.0400 4H29006 08/29/14 08/29/14 1
4H29006-CCV3 Selenium, Dissolved 104 90 110 0.042 0.0400 4H29006 08/29/14 08/29/14 .1
4H29006-CCV3 Silver. Dissolved 107 90 110 0.043 0.0400 4H29006 08/29/14 08/29/14
4H29006-CCV3 Thallium. Dissolved 105 90 110 0.042 0.0400 4H29006 08/29/14 08/29/14 l
Initial Cal Blank-Method EPA 200.8
4H28008-ICB1 Arsenic. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-ICB1 Cadmium. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-ICB1 Chromium. Dissolved 0.0000 4H28008 08/28/14 08/28/14
4H28008-ICB1 Cobalt. Dissolved 0.0000 4H28008 08/28/14 08/28/14 1
4H28008-ICB1 Copper. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-ICB1 Lead. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-ICB1 Molybdenum, Dissolved 0.0000 4H28008 08/28/14 08/28/14 l
4H28008-ICB1 Nickel. Dissolved -0.000 4H28008 08/28/14 08/28/14 1
4H28008-ICB1 Selenium. Dissolved 0.0000 4H28008 08/28/14 08/28/14
4H28008-ICB1 Silver. Dissolved 0.0000 4H28008 08/28/14 08/28/14 J.
4H28008-ICB1 Thallium. Dissolved 0.0000 4H28008 08/28/14 08/28/14 1
4H28008-ICB1 Uranium, Dissolved 0.0000 4H28008 08/28/14 08/28/14 1
Page 14 of 43
QCID Analvte %Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 54 of90 Ana vzed MOl MRl OF
4H28008-ICB1 Vanadium, Dissolved 0.0000 4H28008 08/28/14 08/28/14
4H29006-ICB1 Arsenic, Dissolved 0.0000 4H29006 08/29/14 08/29/14
4H29006-ICB1 Cadmium, Dissolved 0.0000 4H29006 08/29/14 08/29/14
4H29006-ICB1 Lead. Dissolved 0.0000 4H29006 08/29/14 08/29/14
4H29006-ICB1 Molybdenum. Dissolved 0.0003 4H29006 08/29/14 08/29/14 1
4H29006-ICB1 Selenium. Dissolved 0.0000 4H29006 08/29/14 08/29/14
4H29006-ICB1 Silver. Dissolved 0.0002 4H29006 08/29/14 08/29/14
4H29006-ICB1 Thallium, Dissolved 0.0000 4H29006 08/29/14 08/29/14 1
Initial Cal Check -Method EPA 200.8
4H28008-ICV1 Arsenic, Dissolved 99.2 90 110 0.040 0.0400 4H28008 08/28/14 08/28/14
4H28008-ICV1 Cadmium, Dissolved 102 90 110 0.041 0.0400 4H28008 08/28/14 08/28/14 1
4H28008-ICV1 Chromium, Dissolved 97.7 90 110 0.039 0.0400 4H28008 08/28/14 08/28/14
4H28008-ICV1 Cobalt, Dissolved 93.6 90 110 0.037 0.0400 4H28008 08/28/14 08/28/14
4H28008-ICV1 Coooer, Dissolved 99.0 90 110 0.040 0.0400 4H28008 08/28/14 08/28/14 1
4H28008-ICV1 Lead, Dissolved 102 90 110 0.041 0.0400 4H28008 08/28/14 08/28/14 1
4H28008-ICV1 Molybdenum, Dissolved 98.2 90 110 0.039 0.0400 4H28008 08/28/14 08/28/14
4H28008-ICV1 Nickel, Dissolved 99.2 90 110 0.0397 0.0400 4H28008 08/28/14 08/28/14 1
4H28008-ICV1 Selenium, Dissolved 96.7 90 110 0.039 0.0400 4H28008 08/28/14 08/28/14 1 .
4H28008-ICV1 Silver. Dissolved 105 90 110 0.042 0.0400 4H28008 08/28/14 08/28/14
4H28008-ICV1 Thallium, Dissolved 102 90 110 0.041 0.0400 4H28008 08/28/14 08/28/14 l
4H28008-ICV1 Uranium, Dissolved 101 90 110 0.040 0.0400 4H28008 08/28/14 08/28/14 1
4H28008-ICV1 Vanadium, Dissolved 99.0 90 110 0.040 0.0400 4H28008 08/28/14 08/28/14 -
4H29006-ICV1 Arsenic, Dissolved 96.3 90 110 0.039 0.0400 4H29006 08/29/14 08/29/14
4H29006-ICV1 Cadmium, Dissolved 97.7 90 110 0.039 0.0400 4H29006 08/29/14 08/29/14 .
4H29006-ICV1 Lead, Dissolved 98.7 90 110 0.039 0.0400 4H29006 08/29/14 08/29/14 1
4H29006-ICV1 Molybdenum, Dissolved 99.3 90 110 0.040 0.0400 4H29006 08/29/14 08/29/14
Page 15 of 43
QCID Analvte % Rec RPD
4H29006-ICV1 Selenium. Dissolved 94.7
4H29006-ICV1 Silver. Dissolved 108
4H29006-ICV1 Thallium. Dissolved 102
8408836-851 Arsenic. Dissolved 103
8408836-851 Cadmium. Dissolved 96.2
8408836-851 Chromium. Dissolved 98.6
8408836-851 Cobalt, Dissolved 93.6
8408836-851 Copper. Dissolved 98.2
8408836-8Sl Lead, Dissolved 99.2
8408836-851 Molvbdenum. Dissolved 99.4
8408836-8S1 Nickel. Dissolved 102
8408836-851 Selenium. Dissolved 99.0
8408836-851 Sliver. Dissolved 91.7
8408836-8S1 Thallium. Dissolved 101
8408836-851 Uranium. Dissolved 94.8
8408836-8S1 Vanadium, Dissolved 99.3
8408889-8S1 Arsenic. Dissolved 99.8
8408889-8S1 Cadmium. Dissolved 99.1
8408889-851 Lead. Dissolved 98.1
8408889-851 Molybdenum. Dissolved 99.3
8408889-8S1 Selenium. Dissolved 102
8408889-851 Sliver. Dissolved 103
8408889-8S1 Thallium. Dissolved 98.7
8408836-MS1 Arsenic, Dissolved 102
Page 16 of 43
LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch
90 110 0.038 0.0400 4H29006
90 110 0.043 0.0400 4H29006
90 110 0.041 0.0400 4H29006
LCS -Method EPA 200.8
85 115 0.041 0.0400 8408836
85 115 0.038 0.0400 8408836
85 115 0.039 0.0400 8408836
85 115 0.037 0.0400 8408836
85 115 0.039 0.0400 8408836
85 115 0.040 0.0400 8408836
85 115 0.040 0.0400 8408836
85 115 0.0409 0.0400 8408836
85 115 0.040 0.0400 8408836
85 115 0.037 0.0400 8408836
85 115 0.041 0.0400 8408836
85 115 0.038 0.0400 8408836
85 115 0.040 0.0400 8408836
85 115 0.040 0.0400 8408889
85 115 0.040 0.0400 8408889
85 115 0.039 0.0400 8408889
85 115 0.040 0.0400 8408889
85 115 0.041 0.0400 8408889
85 115 0.041 0.0400 8408889
85 115 0.039 0.0400 8408889
Matrix Spike -Method EPA 200.8
70 130 0.082 xXXXXXX-XX 0.0009 0.0800 8408836
Sampled Prepared
Paqe 55 of90
Analyzed MDL MRL OF
08/29/14 08/29/14 1
08/29/14 08/29/14
08/29/14 08/29/14 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00
08/29/14 08/29/14 0.00 0.00 1
08/29/14 08/29/14 0.00 0.00
08/29/14 08/29/14 0.00 0.00 1
08/29/14 08/29/14 0.00 0.00
08/29/14 08/29/14 0.00 0.00
08/29/14 08/29/14 0.00 0.00 1
08/29/14 08/29/14 0.00 0.00
08/28/14 08/28/14 0.00 0.00 1
QCID Analvte % Rec RPD LCL
8408836-MS1 Cadmium, Dissolved 96.3 70
8408836-MS1 Chromium, Dissolved 90.0 70
8408836-MS1 Cobalt. Dissolved 84.4 70
8408836-MS1 Copper, Dissolved 86.9 70
8408836-MS1 Lead, Dissolved 94.3 70
8408836-MS1 Molvbdenum, Dissolved 105 70
8408836-MS1 Nickel. Dissolved 97.1 75
8408836-MS1 Selenium, Dissolved 109 70
8408836-MS1 Silver, Dissolved 87.9 70
8408836-MS1 Thallium, Dissolved 94.2 70
8408836-MS1 Uranium, Dissolved 98.3 70
8408836-MS1 Vanadium, Dissolved 93.0 70
8408836-MS2 Arsenic, Dissolved 94.9 70
8408836-MS2 Cadmium, Dissolved 95.8 70
8408836-MS2 Chromium, Dissolved 98.0 70
B408836-MS2 Cobalt, Dissolved 91.7 70
8408836-MS2 Coooer, Dissolved 95.9 70
B408836-MS2 Lead, Dissolved 96.2 70
B408836-MS2 Molvbdenum, Dissolved 97.6 70
8408836-MS2 Nickel, Dissolved 99.5 75
B408836-MS2 Selenium, Dissolved 92.3 70
8408836-MS2 Silver, Dissolved 92.9 70
8408836-MS2 Thallium, Dissolved 97.1 70
8408836-MS2 Uranium, Dissolved 91.3 70
8408836-MS2 Vanadium, Dissolved 100 70
8408889-MS1 Arsenic, Dissolved 113 70
Page 17 of 43
UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch
130 0.078 XXXXXXX-.XX 0.001 0.0800 8408836
130 o.076 xxxxxxx-xx o.oo4 0.0800 8408836
130 0.076 xxxnxx-xx 0.008 0.0800 8408836
130 0.074 XXX XX XX-XX 0.004 0.0800 8408836
130 0.075 XXXXXXX XX 0 0.0800 8408836
130 0.096 .XXXXXXX X7 0.012 0.0800 8408836
125 0.0856 XXXl\XXX-XX 0.0079 0.0800 8408836
130 0.091 XX \XX)( X -XX 0.003 0.0800 8408836
130 0.070 XXXXXXX XX 0 0.0800 8408836
130 0.076 XXX/XXX-XX 0.0009 0.0800 8408836
130 0.085 XXXXXXX-X'. 0.006 0.0800 8408836
130 0.076 XXXXXXX XX 0.001 0.0800 8408836
130 431 1408830-05 51.2 400 8408836
130 388 1408830-05 4. 72 400 8408836
130 397 1408830-05 4.57 400 8408836
130 408 1408830-05 41.2 400 8408836
130 823 1408830-05 439 400 8408836
130 386 1408830-05 0.870 400 8408836
130 394 1408830-05 3.47 400 8408836
125 497 1408830-05 99.3 400 8408836
130 371 1408830-05 1.44 400 8408836
130 372 1408830-05 0 400 8408836
130 389 1408830-05 0.460 400 8408836
130 447 1408830-05 82.2 400 6408836
130 911 1408830-05 510 400 8408836
130 63.4 1408830-05 58.9 4.00 8408889
Sampled Prepared Paqe 56 of90 Analyzed MDL MRL OF
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.00 0.00
08/28/14 08/28/14 0.00 0.00
08/28/14 08/28/14 0.00 0.00
08/28/14 08/28/14 0.00 0.00
08/28/14 08/28/14 0.00 0.00 1
08/28/14 08/28/14 0.80 5.00 1
08/28/14 08/28/14 0.20 2.00
08/28/14 08/28/14 0.80 5.00 1
08/28/14 08/28/14 0.30 5.00
08/28/14 08/28/14 0.30 10.0
08/28/14 08/28/14 0.40 5.00
08/28/14 08/28/14 0.30 5.00
08/28/14 08/28/14 0. 70 5.00
08/28/14 08/28/14 0.10 5.00
08/28/14 08/28/14 1.00 5.00
08/28/14 08/28/14 0.30 2.00
08/28/14 08/28/14 0.20 5.00 1
08/28/14 08/28/14 0.50 5.00 1
08/29/14 08/29/14 0.00 0.05 1
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 57 of90 Ana vzed MDL MRL OF
8408889-M$1 Cadmium, Dissolved 94.8 70 130 8.47 1408830-05 4.68 4.00 8408889 08/29/14 08/29/14 0.00 0.02 1
8408889-M$1 lead. Dissolved 95.2 70 130 4.80 1408830-05 0.991 4.00 8408889 08/29/14 08/29/14 0.00 0.05 1
8408889-MS1 Molvbdenum. Dissolved 96.1 70 130 7.81 1408830-05 3.97 4.00 8408889 08/29/14 08/29/14 0.00 0.05
8408889-MSl Selenium. Dissolved 113 70 130 6.70 1408830-05 2.17 4.00 B408889 08/29/14 08/29/14 0.00 0.05
B408889-MS1 Silver. Dissolved 96.1 70 130 3.93 1408830-05 0.087 4.00 B408889 08/29/14 08/29/14 0.01 0.05 1
B408889-MS1 Thallium. Dissolved 96.9 70 130 4.40 1408830-05 0.522 4.00 8408889 08/29/14 08/29/14 0.00 0.02 1
Page 18 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 58 of90 Ana vzed MDL MRL OF
Blank -Method EPA 245.1
8409157-BLKl Mercurv. Dissolved -0.000 8409157 09/05/14 09/08/14 0.00 0.00 1
Calibration Blank -Method EPA 245.1
4105022-CCB1 Mercurv. Dissolved 0.0229 4105022 09/05/14 09/08/14
4105022-CCB2 Mercurv. Dissolved 0.0160 4105022 09/05/14 09/08/14
Calibration Check-Method EPA 245.1
4105022-CCV1 Mercurv. Dissolved 106 90 110 5.2800 5.00 4105022 09/05/14 09/08/14 t -
4105022-CCV2 Mercurv. Dissolved 103 90 110 5.1475 5.00 4105022 09/05/14 09/08/14
Initial Cal Blank-Method EPA 245.1
4105022-IC81 Mercurv. Dissolved -0.012 4105022 09/05/14 09/08/14 t
Initial Cal Check-Method EPA 245.1
4105022-ICV1 Mercurv, Dissolved 101 90 110 5.0494 5.00 4105022 09/05/14 09/08/14
LCS-Method EPA 245.1
8409157-851 Mercurv. Dissolved 106 85 115 0.0053 0.00500 8409157 09/05/14 09/08/14 0.00 0.00 1
Matrix Spike -Method EPA 245.1
8409157-MS1 Mercurv. Dissolved 113 75 125 0.0059 1408830-05 0.0002 0.00500 8409157 09/05/14 09/08/14 0.00 0.00 1 -
8409157-MS2 Mercurv, Dissolved 114 75 125 0.0057 ;~x~xxxx xx o 0.00500 8409157 09/05/14 09/08/14 0.00 0.00 1
Matrix Spike Dup -Method EPA 245.1
8409157-MSDl Mercurv. Dissolved 107 5.02 75 125 20 0.0056 1408830-05 0.0002 0.00500 8409157 09/05/14 09/08/14 0.00 0.00 1 .
8409157-MSD2 Mercurv. Dissolved 121 6.06 75 125 20 0.0060 X);;{;IXXX-n 0 0.00500 8409157 09/05/14 09/08/14 0.00 0.00 1
Page 19 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 59 of90 Ana vzed MDL MRL OF
Calibration Blank -Method EPA 300.0
4101001-CCB1 Chloride 0 4101001 08/29/14 08/29/14 1
4101001-CCB1 Fluoride 0,0 4101001 08/29/14 08/29/14 1
4101001-CCB1 Sulfate 0 4101001 08/29/14 08/29/14
4101001-CCB2 Chloride 0 4101001 08/29/14 08/29/14
4101001-CC82 Fluoride 0.0 4101001 08/29/14 08/29/14 1 -
4101001-CC82 Sulfate 0 4101001 08/29/14 08/29/14 -
4101001-CC83 Chloride 0 4101001 08/29/14 08/29/14 l
4101001-CCB3 Fluoride 0.0 4101001 08/29/14 08/29/14 1 .
4101001-CC83 Sulfate 0.7 4101001 08/29/14 08/29/14
Calibration Check-Method EPA 300.0
4101001-CCV1 Chloride 100 90 110 20 20.0 4101001 08/29/14 08/29/14 .
4101001-CCV1 Fluoride 100 90 110 2.0 2.00 4101001 08/29/14 08/29/14 1
4101001-CCV1 Sulfate 100 90 110 40 40.0 4101001 08/29/14 08/29/14 1 .
4101001-CCV2 Chloride 100 90 110 20 20.0 4101001 08/29/14 08/29/14 l .
4101001-CCV2 Fluoride 95.0 90 110 1.9 2.00 4101001 08/29/14 08/29/14 1 -
4101001-CCV2 Sulfate 100 90 110 40 40.0 4101001 08/29/14 08/29/14 1
4101001-CCV3 Chloride 100 90 110 20 20.0 4101001 08/29/14 08/29/14 1 -
4101001-CCV3 Fluoride 95.0 90 110 1.9 2.00 4101001 08/29/14 08/29/14
4101001-CCV3 Sulfate 102 90 110 41 40.0 4101001 08/29/14 08/29/14
LCSW-Method EPA 300.0
8408926-851 Chloride 102 90 110 51 50.0 8408926 08/29/14 08/29/14 0.07 1 1 -
8408926-BS1 Fluoride 100 90 110 5.0 5.00 8408926 08/29/14 08/29/14 0.02 0.1 1
8408926-BS1 Sulfate 100 90 110 100 100 8408926 08/29/14 08/29/14 0.2 1 1 -
8408926-852 Chloride 102 90 110 51 50.0 8408926 08/29/14 08/29/14 0.07 1
8408926-852 Fluoride 98.0 90 110 4.9 5.00 8408926 08/29/14 08/29/14 0.02 0.1
Page 20 of 43
QCID
B408926-BS2
B408926-BSD1
B408926-BSD1
B408926-BSD1
B408926-8SD2
8408926-8502
8408926-BSD2
8408926-MS1
8408926-MS1
A-01-
B408926-MS1
8408926-M$2
Analvte
Sulfate
Chloride
Fluoride
Sulfate
Chloride
Fluoride
Sulfate
Chloride
Fluoride
Sulfate
Chloride
% Rec RPD
100
102 0.00
98.0 2.02
100 0.00
102 0.00
96.0 2.06
100 0.00
100
96.0
100
100
LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch
90 110 100 100 B408926
LCSW Dup -Method EPA 300.0
90 110 20 51 50.0 8408926
90 110 20 4.9 5.00 B408926
90 110 200 100 100 B408926
90 110 20 51 50.0 B408926
90 110 20 4.8 5.00 8408926
90 110 200 100 100 8408926
Matrix Spike -Method EPA 300.0
80 120 9200 1408830-05 4200 5000 B408926
80 120 1800 1408830-05 1320 500 B408926
80 120 66000 1408830-05 56000 10000 B408926
80 120 5200 1408830-05 4200 1000 8408926
Samoled Prepared Paqe 60 of90 Analvzed MOL MRL OF
08/29/14 08/29/14 0.2 1 1
08/29/14 08/29/14 0.07
08/29/14 08/29/14 0.02 0.1
08/29/14 08/29/14 0.2 1 1
08/29/14 08/29/14 0.07 1 1
08/29/14 08/29/14 0.02 0.1 1
08/29/14 08/29/14 0.2
08/29/14 08/29/14 35 500 500
08/29/14 08/29/14 10.0 50.0 500
08/29/14 08/29/14 100 500 500
08/29/14 08/29/14 7 100 100
B408926-MS2 Fluoride 80.0 80 120 1400 1408830-05 1320 100 8408926 08/29/14 08/29/14 2.0 10.0 100
A-01-
8408926-M$2 Sulfate -10.0 80 120 55800 1408830-05 56000 2000 8408926 08/29/14 08/29/14 20 100 100
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
8408926-MSDl
B408926-MSD1
A-01-
8408926-MSDl
8408926-MSD2
8408926-MSD2
A-01-
Chloride
Fluoride
Sulfate
Chloride
Fluoride
Matrix Spike Dup-Method EPA 300.0
102 1.08 80 120 20 9300 1408830-05 4200 5000 B408926 08/29/14 08/29/14 35 500 500
98.0 0.554 80 120 20 1810 1408830-05 1320 500 B408926 08/29/14 08/29/14 10.0 50.0 500
100 0.00 80 120 20 66000 1408830-05 56000 10000 B408926 08/29/14 08/29/14 100 500 500
100 0.00 80 120 20 5200 1408830-05 4200 1000 B408926 08/29/14 08/29/14 7 100 100
80.0 0.00 80 120 20 1400 1408830-05 1320 100 B408926 08/29/14 08/29/14 2.0 10.0 100
8408926-MSD2 Sulfate -5.00 0.179 80 120 20 55900 1408830-05 56000 2000 8408926 08/29/14 08/29/14 20 100 100
QM-4X-The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and/or LCSD
recoveries within the acceptance limits.
PBW -Method EPA 300.0
B408926-BLK1 Chloride 03 B408926 08/29/14 08/29/14 0.07 1 1
B408926-BLK1 Fluoride 0.0 B408926 08/29/14 08/29/14 0.02 0.1 1
Page 21 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 61 of90 Ana vzed MDL MRL OF
8408926-BLKl Sulfate 0.7 8408926 08/29/14 08/29/14 0.2 1 1
B408926-BLK2 Chloride 0 8408926 08/29/14 08/29/14 0.07 1
B408926-BLK2 Fluoride 0.0 8408926 08/29/14 08/29/14 0.02 0.1
B408926-BLK2 Sulfate 0 8408926 08/29/14 08/29/14 0.2 1 1
Page 22 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch
Blank-Method EPA 353.2
8409111-8LK1 Nitrate+ Nitrite, Total 0.04 8409111
Calibration Blank-Method EPA 353.2
4104015-CCB1 Nitrate+ Nitrite, Total 0.01 4104015
4104015-CCB2 Nitrate+ Nitrite, Total 0.02 4104015
4104015-CC83 Nitrate+ Nitrite, Total 0.03 4104015
Calibration Check-Method EPA 353.2
4104015-CCV1 Nitrate+ Nitrite, Total 94.0 90 110 0.9 1.00 4104015
4104015-CCV2 Nitrate+ Nitrite, Total 95.0 90 110 1.0 1.00 4104015
4104015-CCV3 Nitrate+ Nitrite, Total 95.0 90 110 1.0 1.00 4104015
Initial Cal Blank-Method EPA 353.2
4104015-IC81 Nitrate+ Nitrite, Total 0.03 4104015
Initial Cal Check -Method EPA 353.2
4104015-ICV1 Nitrate+ Nitrite, Total 94.0 90 110 0.9 1.00 4104015
LCS -Method EPA 353.2
8409111-651 Nitrate+ Nitrite, Total 97.0 90 110 1.9 2.00 8409111
Matrix Spike-Method EPA 353.2
Sampled Prepared Paoe 62 of90 Analyzed MDL MRL DF
09/04/14 09/04/14 0.03 0.1 1
09/04/14 09/04/14 1
09/04/14 09/04/14 1
09/04/14 09/04/14 1
09/04/14 09/04/14 l
09/04/14 09/04/14 1
09/04/14 09/04/14 1
09/04/14 09/04/14 1
09/04/14 09/04/14
09/04/14 09/04/14 0.03 0.1 1
B409111-MS1 Nitrate+ Nitrite, Total 77.0 80 120 30.6 ;'X\XXY>;-X': 15.2 20.0 8409111 09/04/14 09/04/14 0.6 2.0 20
QM-05-The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The analytical batch was accepted based on the acceptable data provided by the laboratory Control Sample(s) [LCS]
and/or LCS Duplicates.
B409111-MS2 Nitrate+ Nitrite, Total 76.0 80 120 115 1408830-05 39.0 100 8409111 09/04/14 09/04/14 3.0 10.0 100
Matrix Spike Dup -Method EPA 353.2
8409111-MSD1 Nitrate + Nitrite, Total 92.0 9.35 80 120 20 33.6 :(X~XXXX X~ 15.2 20.0 8409111 09/04/14 09/04/14 0.6 2.0 20
B409111-MSD2 Nitrate+ Nitrite, Total 87.0 9.13 80 120 20 126 1408830-05 39.0 100 8409111 09/04/14 09/04/14 3.0 10.0 100
QM-05-The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The analytical batch was accepted based on the acceptable data provided by the Laboratory Control Sample(s) [LCS]
and/or LCS Duplicates.
Page 23 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 63 of90 Ana vzed MDL MRL OF
Blank -Method EPA 82608
B408858-BLK1 1.1.1.2-Tetrachloroethane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-BLK1 1.1.1-Trichloroethane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0
B408858-BLK1 1,1.2,2-Tetrachloroethane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0
9408858-BLK1 1.1.2-Trlchloroethane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0
8408858-8LK1 1,1, 2-Trich lorotrifluoroethan e 0.00 Yes 9408858 08/27/14 08/27/14 0.3 1.0 1
8408858-9LK1 1.1-Dichloroethane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-9LK1 1,1-Dichloroethene 0.00 Yes 9408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 1,1-Dichloroorooene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0
9408858-8LK1 1,2,3-Trichlorobenzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0
8408858-8LK1 1,2,3-Trichloroorooane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 1.2.4-Trlch lorobenzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 1.2.4-Trlmethvlbenzene 0.00 Yes 9408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 1,2-Dibromo-3-chloroorooane 0.00 Yes 8408858 08/27/14 08/27/14 1.0 1.0 1
8408858-8LK1 1,2-Dibromoethane (ED8l 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 1,2-Dichlorobenzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 1.2-Dichloroethane 0.00 Yes 9408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 1,2-Dichloroethane-d4 109 70 130 10.9 10.0 'Yes 9408858 08/27/14 08/27/14 1
9408858-8LK1 1.2-Dichloroorooane 0.00 Yes 9408858 08/27/14 08/27/14 0.3 1.0
8408858-8LK1 1.3.5-Trimethvlbenzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-9LK1 1,3-Dichlorobenzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
9408858-9LK1 1.3-Dichloropropane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 1.4-Dichlorobenzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 2.2-Dichloroprooane 0.00 Yes 9408858 08/27/14 08/27/14 0.3 1.0 1
9408858-8LK1 2-Chlorotoluene 0.00 Yes 9408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 2-Nltroprooane 0.00 Yes 8408858 08/27/14 08/27/14 10.0 10.0
Page 24 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 64 of90 Ana vzed MDL MRL OF
6408858-6LK1 4-6romofluorobenzene 106 70 130 10.6 10.0 Yes 8408858 08/27/14 08/27/14 1
6408858-6LK1 4-Chlorotoluene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0
B408858-6LK1 4-lsoproovltoluene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0
8408858-8LK1 Acetone 0.00 Yes 8408858 08/27/14 08/27/14 10.0 10.0 .
8408858-BLK1 Acrvlonltrile 0.00 Yes 8408858 08/27/14 08/27/14 10.0 10.0 1
B408858-BLK1 Benzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 Bromobenzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-BLK1 Bromochloromethane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1 .
8408858-BLK1 8romodichloromethane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 Bromoform 0.00 Yes 8408858 08/27/14 08/27/14 1.0 1.0 1
8408858-BLK1 Bromo methane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 Carbon Disulfide 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
B408858-8LK1 Carbon Tetrachloride 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 Chlorobenzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 Chloroethane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-6LK1 Chloroform 0.00 Yes 8408858 08/27/14 08/27/14 1.0 1.0 1
B408858-6LK1 Chloromethane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 cis-1.2-Dichloroethene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-6LK1 cis-1.3-Dichloroorooene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 Cvclohexanone 0.00 Yes 8408858 08/27/14 08/27/14 20.0 20.0 1
B408858-BLK1 Dibromochloromethane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 Dibromomethane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
B408858-8LK1 Dichlorodifluoromethane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 Ethvl Acetate 0.00 Yes 8408858 08/27/14 08/27/14 10.0 10.0 1
B408858-BLK1 Ethvl Ether 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-8LK1 Ethvlbenzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
Page 25 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 65 of90 Ana vzed MDL MRL OF
B408858-BLK1 Hexachlorobutadlene 0.00 Yes B408858 08/27/14 08/27/14 0.3 1.0 1 -
B408858-BLK1 lsobutanol 0.00 Yes B408858 08/27/14 08/27/14 10.0 10.0
B408858-BLK1 lsooroovlbenzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0
B408858-BLK1 Methvl Ethvl Ketone 0.00 Yes 8408858 08/27/14 08/27/14 10.0 10.0
B408858-BLK1 Methvllsobutvl Ketone 0.00 Yes B408858 08/27/14 08/27/14 10.0 10.0 1
B408858-BLK1 Methvlene Chloride 0.00 Yes 8408858 08/27/14 08/27/14 1.0 1.0 1
B408858-BLK1 Methvl-tert-butvl ether (MTBE\ 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 Naohthalene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 n-Butvl Alcohol 0.00 Yes 8408858 08/27/14 08/27/14 40.0 40.0 1
B408858-BLK1 n-Butvlbenzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 Nitrobenzene 0.00 Yes 8408858 08/27/14 08/27/14 20.0 20.0 1
B408858-BLK1 n-Proovl Benzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 o-lsooroovltoluene 0.00 Yes B408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 sec-Butvl Benzene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 Stvrene 0.00 Yes 8408858 08/27/14 08/27/14 1.0 1.0 1
8408858-BLK1 tert-Butvlbenzene 0.00 Yes 8408858 08/27/14 08/27/14 1.0 1.0 1
8408858-BLK1 Tetrachloroethene 0.00 Yes B408858 08/27/14 08/27/14 0.3 1.0 1 .
8408858-8LK1 Toluene 0.00 Yes B408858 08/27/14 08/27/14 0.3 1.0 1 -
B408858-BLK1 Toluene-dB 101 70 130 10.1 10.0 Yes B408858 08/27/14 08/27/14 1 .
B408858-BLK1 trans-1.2-Dichloroethene 0.00 Yes B408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 trans-1,3-Dichloroorooene 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-BLK1 Trichloroethene 0.00 Yes B408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 Trichlorofluoromethane 0.00 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 Vinvl Chloride 0.00 Yes B408858 08/27/14 08/27/14 0.3 1.0 1
B408858-BLK1 Xvlenes. total 0.00 Yes B408858 08/27/14 08/27/14 0.3 1.0 1
B408909-BLK1 1,1,1.2-Tetrachloroethane 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
Page 26 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 66 of90 Ana vzed MDL MRL OF
B408909-8LK1 1.1.1-Trichloroethane 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0
8408909-8LK1 1.1.2.2-Tetrachloroethane 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 1.1.2-Trichloroethane 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 1.1.2-Trich Jorotrifl uoroetha ne 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0
8408909-8LK1 1.1-Dichloroethane 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 1.1-Dichloroethene 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0
8408909-8LK1 1.1-Dichloropropene 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 1,2.3-Trichlorobenzene 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0
8408909-8LK1 1,2,3-Trichloroorooane 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 1.2.4-Trichlorobenzene 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 1.2.4-Trimethvlbenzene 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 1.2-Dibromo-3-chloropropane 0.00 Yes 6408909 08/28/14 08/28/14 1.0 1.0 1
8408909-8LK1 1.2-Dibromoethane (ED8) 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
6408909-8LK1 1.2-Dichlorobenzene 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 1.2-Dichloroethane 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 1.2-Dichloroethane-d4 110 70 130 11.0 10.0 Yes 6408909 08/28/14 08/28/14 1
8408909-8LK1 1.2-Dichloroorooane 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0
8408909-8LK1 1.3.5-Trimethvlbenzene 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 1,3-Dichlorobenzene 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 1.3-Dichloroorooane 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 1.4-Dichlorobenzene 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 2.2-Dichloroorooane 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 2-Chlorotoluene 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 2-Nitropropane 0.00 Yes 8408909 08/28/14 08/28/14 10.0 10.0 1
8408909-8LK1 4-8romofluorobenzene 108 70 130 10.8 10.0 Yes 8408909 08/28/14 08/28/14 1
6408909-8LK1 4-Chlorotoluene 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0
Page 27 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Sok Value Surr? Batch Sampled Prepared Pa~e 67 of90 Ana vzed MDL MRL OF
B408909-BLK1 4-lsooroovltoluene 0.00 Yes B408909 08/28/14 08/28/14 0.3 1.0 1
B408909-8LK1 Acetone 0.00 Yes B408909 08/28/14 08/28/14 10.0 10.0
8408909-8LK1 Acrvlonitrile 0.00 Yes B408909 08/28/14 08/28/14 10.0 10.0 1 -
B408909-8LK1 Benzene 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
B408909-BLK1 8romobenzene 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 Bromochloromethane 0.00 Yes B408909 08/28/14 08/28/14 0.3 1.0 1
B408909-8LK1 Bromodichloromethane 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0
B408909-8LK1 Bromoform 0.00 Yes B408909 08/28/14 08/28/14 1.0 1.0 1
B408909-BLK1 Bromomethane 0.00 Yes B408909 08/28/14 08/28/14 0.3 1.0 1
B408909-BLK1 Carbon Disulfide 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-BLKl Carbon Tetrachloride 0.00 Yes B408909 08/28/14 08/28/14 0.3 1.0 1
B408909-BLK1 Chlorobenzene 0.00 Yes B408909 08/28/14 08/28/14 0.3 1.0
B408909-BLK1 Chloroethane 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
B408909-8LK1 Chloroform 0.00 Yes B408909 08/28/14 08/28/14 1.0 1.0 1
B408909-BLK1 Chloromethane 0.00 Yes B408909 08/28/14 08/28/14 0.3 1.0 1
B408909-BLK1 cis-1.2-Dichloroethene 0.00 Yes B408909 08/28/14 08/28/14 0.3 1.0 1
B408909-BLK1 cis-1.3-Dichloroorooene 0.00 Yes B408909 08/28/14 08/28/14 0.3 1.0 1
B408909-BLK1 Cvclohexanone 0.00 Yes B408909 08/28/14 08/28/14 20.0 20.0 1
B408909-BLK1 Dibromochloromethane 0.00 Yes B408909 08/28/14 08/28/14 0.3 1.0 1
B408909-BLK1 Dibromomethane 0.00 Yes B408909 08/28/14 08/28/14 0.3 1.0 1
B408909-8LK1 Dichlorodifluoromethane 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-BLK1 Ethvl Acetate 0.00 Yes 8408909 08/28/14 08/28/14 10.0 10.0 .
B408909-6LK1 Ethvl Ether 0.00 Yes B408909 08/28/14 08/28/14 0.3 1.0 1
6408909-BLKl Ethvlbenzene 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
6408909-BLKl Hexachlorobutadiene 0.00 Yes B408909 08/28/14 08/28/14 0.3 1.0 1 .
6408909-6LK1 lsobutanol 0.00 Yes B408909 08/28/14 08/28/14 10.0 10.0 1
Page 28 of 43
QCID Analvte %Ret RPD LCL UCL RPD MaK Result QC Source Source Cone Sok Value Surr? Batch Sampled Prepared Pa~e 68 of90 Ana vzed MDL MRL OF
8408909-BLK1 lsoorocvlbenzene 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 Methvl Ethvl Ketone 0.00 Yes 8408909 08/28/14 08/28/14 10.0 10.0 1
B408909-8LK1 Methvllsobutvl Ketone 0.00 Yes 8408909 08/28/14 08/28/14 10.0 10.0 1
B408909-8LK1 Methvlene Chloride 0.00 Yes B408909 08/28/14 08/28/14 1.0 1.0 1
B408909-BLK1 Methvl-tert-butvl ether fMTBEl 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-BLK1 Naohthalene 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
B408909-BLK1 n-Butvl Alcohol 0.00 Yes 8408909 08/28/14 08/28/14 40.0 40.0 1
8408909-BLK1 n-Butvlbenzene 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 Nitrobenzene 0.00 Yes 8408909 08/28/14 08/28/14 20.0 20.0 1
B408909-8LK1 n-Propvl Benzene 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-BLK1 c-lsocropvltoluene 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
6408909-8LK1 sec-6utvl Benzene 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
B408909-8LK1 Stvrene 0.00 Yes B408909 08/28/14 08/28/14 1.0 1.0 1
8408909-BLK1 tert-Butvlbenzene 0.00 Yes 8408909 08/28/14 08/28/14 1.0 1.0 1
8408909-8LK1 Tetrachloroethene 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 Toluene 0.68 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1 .
8408909-8LK1 Toluene-dB 102 70 130 10.2 10.0 Yes 8408909 08/28/14 08/28/14 1 -
8408909-BLK1 trans-1.2-Dichloroethene 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 trans-1.3-Dichlorocrooene 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 Trichloroethene 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1 -
8408909-8LK1 Trichlorofluoromethane 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-8LK1 Vinyl Chloride 0.00 Yes 8408909 08/28/14 08/28/14 0.3 1.0 1
8408909-6LK1 Xvlenes, total 0.00 Yes 6408909 08/28/14 08/28/14 0.3 1.0 1
LCS-Method EPA 82608
8408858-851 1.1-Dichloroethene 81.5 70 130 8.15 10.0 Yes 8408858 08/27/14 08/27/14 0.3 1.0 1
8408858-851 1.2-Dichloroethane-d4 106 70 130 10.6 10.0 Yes 8408858 08/27/14 08/27/14
Page 29 of 43
QCID Analvte %Ret RPD
8408858-851 4-Bromofluorobenzene 105
840B85B-8S1 Benzene 96.2
840885B-BS1 Ch lorobenzene 93.4
B40B858-BS1 Toluene 95.0
B408858-BS1 Toluene-dB 101
8408858-851 Trichloroethene 94.3
B40B909-B51 1.1-Dichloroethene B0.5
B40B909-BS1 1,2-Dichloroethane-d4 110
B408909-B51 4-Bromofluorobenzene 105
B408909-B51 Benzene 99.8
B408909-B51 Chlorobenzene 94.5
B40B909-BS1 Toluene 10B
B40B909-BS1 Toluene-dB 102
B40B909-BS1 Trichloroethene 96.7
B40BB5B-MS1 1.1-Dichloroethene 81.5
B40BB5B-MS1 1.2-Dichloroethane-d4 103
B408858-MS1 4-Bromofluorobenzene 103
B408858-MS1 Benzene 99.7
B408858-MS1 Chlorobenzene 96.4
8408B58-M51 Toluene 97.4
840BB58-MS1 Toluene-dB 101
B408858-M51 Trichloroethene 96.4
B408909-MS1 1.1-Dichloroethene B8.2
B408909-M51 1.2-Dichloroethane-d4 120
B408909-MS1 4-Bromofluorobenzene 107
Page 30 of 43
LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch
70 130 10.5 10.0 Yes 8408858
70 130 9.62 10.0 Yes B408B58
70 130 9.34 10.0 Yes 8408858
70 130 9.50 10.0 Yes 8408858
70 130 10.1 10.0 Yes 8408858
70 130 9.43 10.0 Yes 8408858
70 130 B.05 10.0 Yes 8408909
70 130 11.0 10.0 Yes 8408909
70 130 10.5 10.0 Yes 8408909
70 130 9.98 10.0 Yes 8408909
70 130 9.45 10.0 Yes 8408909
70 130 10.B 10.0 Yes B408909
70 130 10.2 10.0 Yes B408909
70 130 9.67 10.0 Yes B408909
Matrix Spike -Method EPA 82608
70 130 40.8 XXXXXXX-XX 0 50.0 Yes 840885B
70 130 51.4 XXX>:/XX-XX 50.0 Yes 8408858
70 130 51.7 XXXXXXX-XX 50.0 Yes 8408858
70 130 49.8 XXXXXXX-XX 0 50.0 Yes 8408858
70 130 48.2 x~xxxxx-xx o 50.0 Yes 8408858
70 130 48.7 XXXXXXX·XX 0 50.0 Yes 8408858
70 130 50.4 x;,x; XXX· XX 50.0 Yes 8408858
70 130 48.2 XXXXXXX-XX 0 50.0 Yes 8408858
70 130 44.1 1408830-05 0 50.0 Yes B408909
70 130 59.B 1408830-05 50.0 Yes 8408909
70 130 53.4 1408830-05 50.0 Yes 840B909
Sampled Prepared Paqe 69 of90 Analyzed MDL MRL DF
OB/27/14 08/27/14 1
08/27/14 08/27/14 0.3 1.0 1
OB/27/14 08/27/14 0.3 1.0 1
08/27/14 08/27/14 0.3 1.0 1
08/27/14 08/27/14 1
08/27/14 08/27/14 0.3 1.0 1
OB/28/14 OB/2B/14 0.3 1.0 1
08/28/14 08/28/14 1
08/2B/14 08/28/14 1
08/28/14 08/28/14 0.3 1.0 1
08/2B/14 08/28/14 0.3 1.0 1
08/28/14 08/28/14 0.3 1.0 1
08/28/14 08/28/14 1
08/28/14 08/28/14 0.3 1.0 1
08/27/14 08/27/14 1.5 5.0 1
08/27/14 08/27/14 1
08/27/14 08/27/14 1
08/27/14 08/27/14 1.5 5.0 1
08/27/14 08/27/14 1.5 5.0
08/27/14 08/27/14 1.5 5.0 1
08/27/14 08/27/14 1
08/27/14 08/27/14 1.5 5.0
08/28/14 08/28/14 1.5 5.0 1
08/28/14 08/28/14 1
08/28/14 08/28/14 1
QCID Analvte
B408909-MS1 Benzene
B408909-MS1 Chlorobenzene
B408909-MS1 Toluene
B408909-MS1 Toluene-dB
B408909-MS1 Trichloroethene
B408909-MS2 1.1-Dichloroethene
B408909-MS2 1,2-Dichloroethane-d4
B408909-MS2 4-Bromofluorobenzene
B408909-MS2 Benzene
B408909-MS2 Chlorobenzene
B408909-MS2 Toluene
B408909-MS2 Toluene-dB
8408909-MS2 Trichloroethene
8408858-MSD1 1.1-Dichloroethene
8408858-MSD1 1.2-Dichloroethane-d4
B408858-MSD1 4-Bromofluorobenzene
8408858-MSD1 Benzene
B408858-MSD1 Ch lorobenzene
B408858-MS01 Toluene
B408858-MSD1 Toluene-dB
B408858-MSD1 Trichloroethene
B408909-MSD1 1.1-Dichloroethene
B408909-MSD1 1,2-0ichloroethane-d4
B408909-MS01 4-Bromofluorobenzene
8408909-MS01 Benzene
Page 31 of 43
% Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch
107 70 130 53.4 1408830-05 0 50.0 Yes 8408909
101 70 130 50.4 1408830-05 0 50.0 Yes 8408909
109 70 130 56.2 1408830-05 1.85 50.0 Yes 8408909
102 70 130 51.1 1408830-05 so.o Yes 8408909
102 70 130 51.0 1408830-05 0 50.0 Yes 8408909
88.3 70 130 44.2 XXXXXXX-XX 0 50.0 Yes 8408909
106 70 130 53.2 '<XXXXXX-XX 50.0 Yes 8408909
106 70 130 53.1 XXXXXXX·XX 50.0 Yes 8408909
106 70 130 52.8 XXXXXXX XX 0 50.0 Yes 8408909
99.2 70 130 49.6 XXXXXXX-XX 0 50.0 Yes 8408909
113 70 130 56.9 XXXXXXX-XX 0.53 50.0 Yes 8408909
102 70 130 50.8 xxxxxxx-xx 50.0 Yes 8408909
102 70 130 51.0 XXXXXXX-XX 0 50.0 Yes 8408909
Matrix Spike Dup -Method EPA 82608
83.6 2.54 70 130 20 41.8 XXXXXXX-XX 0 50.0 Yes 8408858
106 70 130 53.0 XXXXXXX-XX 50.0 Yes 8408858
105 70 130 52.4 xxxxxxx-xx 50.0 Yes 8408858
103 3.06 70 130 20 51.4 XXXXXXX-XX 0 50.0 Yes 8408858
99.1 2.76 70 130 20 49.6 XXXXXXX-XX 0 50.0 Yes 8408858
102 4.12 70 130 20 50.8 XXXXXXX·XX 0 50.0 Yes 8408858
102 70 130 50.8 XXXXXXX-XX 50.0 Yes 8408858
99.2 2.86 70 130 20 49.6 XXXXXXX-XX 0 50.0 Yes 8408858
88.4 0.227 70 130 20 44.2 1408830-05 0 50.0 Yes 8408909
120 70 130 60.0 1408830-05 50.0 Yes 8408909
106 70 130 53.2 1408830-05 50.0 Yes 8408909
106 0.845 70 130 20 53.0 1408830-05 0 50.0 Yes 8408909
Sampled Prepared PaQe 70 of90 Analyzed MDL MRL OF
08/28/14 08/28/14 1.5 5.0 1
08/28/14 08/28/14 1.5 5.0
08/28/14 08/28/14 1.5 5.0
08/28/14 08/28/14 1
08/28/14 08/28/14 1.5 5.0 1
08/28/14 08/28/14 1.5 5.0 1
08/28/14 08/28/14
08/28/14 08/28/14 1
08/28/14 08/28/14 1.5 5.0
08/28/14 08/28/14 1.5 5.0 1
08/28/14 08/28/14 1.5 5.0 1
08/28/14 08/28/14 1
08/28/14 08/28/14 1.5 5.0 1
08/27/14 08/27/14 1.5 5.0 1
08/27/14 08/27/14 1
08/27/14 08/27/14 1
08/27/14 08/27/14 1.5 5.0 1
08/27/14 08/27/14 1.5 5.0
08/27/14 08/27/14 1.5 5.0 1
08/27/14 08/27/14 1
08/27/14 08/27/14 1.5 5.0 1
08/28/14 08/28/14 1.5 5.0 1
08/28/14 08/28/14 1
08/28/14 08/28/14 1
08/28/14 08/28/14 1.5 5.0 1
QCID Analvte %Rec RPD LCL UCL RPD Max Result QC Source Source Conc Spk Value Surr? Batch Sampled Prepared Pa~ 71 of90 Ana zed MDL MRL DF
8408909·MSD1 Chtorobenzene 98.9 1.80 70 130 20 49.4 1408830-05 0 50.0 Yes 8408909 08/28/14 08/28/14 1.5 5.0 1
8408909·MSD1 Toluene 108 0.831 70 130 20 55.8 1408830-05 1.85 50.0 Yes 8408909 08/28/14 08/28/14 1.5 5.0 1
B408909-MSD1 Toluene-dB 102 70 130 50.8 1408830-05 50.0 Yes 8408909 08/28/14 08/28/14 1
8408909-MSD1 Trichloroethene 99.2 2.78 70 130 20 49.6 1408830-05 0 50.0 Yes 8408909 08/28/14 08/28/14 1.5 5.0 1
Page 32 of43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 72 of90 Ana vzed MDL MRL OF
Blank -Method EPA 82700
6408660-6LK1 1,2,4-Trichlorobenzene 0 Yes 6408660 08/22/14 08/27/14 1 5 1
B408660-6LK1 1,2-Dichlorobenzene 0 Yes 8408660 08/22/14 08/27/14 2 5 1
6408660-6LK1 1.2-Diohenvlhvdrazine 0 Yes 8408660 08/22/14 08/27/14 2 10 1
B408660-6LK1 1,3-Dichlorobenzene 0 Yes 6408660 08/22/14 08/27/14 1 5 1
B408660-6LK1 1.4-Dichlorobenzene 0 Yes 6408660 08/22/14 08/27/14 0. 7 5 1
6408660-6LK1 2,3.4,6-Tetrachloroohenol 0 Yes 8408660 08/22/14 08/27/14 2 10 1
6408660-6LK1 2,4,5-Trichloroohenol 0 Yes 8408660 08/22/14 08/27/14 3 10 1
B408660-BLK1 2,4,6-Tribromoohenol 58.0 20 130 58.0 100 Yes 8408660 08/22/14 08/27/14 1
B408660-BLK1 2,4,6-Trichlorophenol 0 Yes 8408660 08/22/14 08/27/14 1 10 1
8408660-8LK1 2,4-Dich loroohenol 0 Yes 8408660 08/22/14 08/27/14 0.9 10 1
8408660-8LK1 2.4-Dimethvlohenol 0 Yes 8408660 08/22/14 08/27/14 1 10 1
8408660-8LK1 2.4-Dinitroohenol 0 Yes 8408660 08/22/14 08/27/14 4 10 1
8408660-6LK1 2.4-Dinitrotoluene 0 Yes 8408660 08/22/14 08/27/14 0.8 5 1
8408660-8LK1 2,6-Dichloroohenol 0 Yes 8408660 08/22/14 08/27/14 2 10 1
8408660-6LK1 2,6-Dinitrotoluene 0 Yes 8408660 08/22/14 08/27/14 0.9 5 1
8408660-6LK1 2-Chloronaohthalene 0 Yes 8408660 08/22/14 08/27/14 0.6 5 1
8408660-6LK1 2-Chloroohenol 0 Yes 8408660 08/22/14 08/27/14 2 10 1
8408660-6LK1 2-Fiuorobiohenvl 52.0 37 130 26.0 50.0 Yes 6408660 08/22/14 08/27/14
6408660-8LK1 2-Fiuoroohenol 48.0 15 130 48.0 100 Yes 8408660 08/22/14 08/27/14 1
8408660-6LK1 2-Methvlnaohthalene 0 Yes 8408660 08/22/14 08/27/14 2 5 1
6408660-6LK1 2-Methvlohenol 0 Yes 8408660 08/22/14 08/27/14 1 10
6408660-6LK1 2-Nitroaniline 0 Yes 8408660 08/22/14 08/27/14 1 5 1 .
8408660-6LK1 2-Nitroohenol 0 Yes 8408660 08/22/14 08/27/14 2 10 1 .
6408660-6LK1 3 & 4-Methvlohenol 0 Yes 8408660 08/22/14 08/27/14 2 10 1
6408660-6LK1 3,3' -Dichlorobenzidine 0 Yes 6408660 08/22/14 08/27/14 2 10
Page 33 of 43
QCID Analvte %Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 73 of90 Ana vzed MDL MRL OF
B408660-BLK1 3-Nitroaniline 0 Yes 8408660 08/22/14 08/27/14 0.9 5 .l
B408660-BLK1 4,6-Dinitro-2-methvlohenol 0 Yes 8408660 08/22/14 08/27/14 1 10 .l
B408660-BLK1 4-Bromoohenvl ohenvl ether 0 Yes 8408660 08/22/14 08/27/14 1 5 1
B408660-BLK1 4-Chloro-3-methvlohenol 0 Yes 8408660 08/22/14 08/27/14 2 10 1
B408660-BLK1 4-Chloroaniline 0 Yes 8408660 08/22/14 08/27/14 0.8 5 1
B408660-BLK1 4-Chloroohenvl Phenvl Ether 0 Yes 8408660 08/22/14 08/27/14 0.6 5 1
B408660-BLK1 4-Nitroaniline 0 Yes 8408660 08/22/14 08/27/14 2 5
B408660-BLK1 4-Nitroohenol 0 Yes 8408660 08/22/14 08/27/14 4 10 l
8408660-BLK1 Acenaohthene 0 Yes 8408660 08/22/14 08/27/14 2 5 1
8408660-BLKl Acenaohthvlene 0 Yes 8408660 08/22/14 08/27/14 0.5 5 1
B408660-8LK1 Aniline 0 Yes 8408660 08/22/14 08/27/14 0.9 5 1
8408660-BLK1 Anthracene 0 Yes 8408660 08/22/14 08/27/14 0. 7 5 l .
B408660-BLK1 Azobenzene 0 Yes 8408660 08/22/14 08/27/14 2 5 1
8408660-BLK1 8enzo (al anthracene 0 Yes 8408660 08/22/14 08/27/14 0.9 5 1
8408660-BLK1 Benzo (al ovrene 0 Yes 8408660 08/22/14 08/27/14 0.9 5 1
8408660-BLK1 Benzo (bl fluoranthene 0 Yes 8408660 08/22/14 08/27/14 1 5 1
B408660-BLK1 Benzo hz.h.il oervlene 0 Yes 8408660 08/22/14 08/27/14 2 5 1
8408660-BLK1 Benzo (kl fluoranthene 0 Yes 8408660 08/22/14 08/27/14 1 5 1
B408660-BLK1 Benzoic acid 0 Yes 8408660 08/22/14 08/27/14 2 10 1
B408660-8LK1 8enzvl Alcohol 0 Yes 8408660 08/22/14 08/27/14 1 5 1
8408660-8LK1 81s (2-chloroethoxvl Methane 0 Yes 8408660 08/22/14 08/27/14 0. 7 5 1
8408660-BLK1 Bis (2-chloroethvll Ether 0 Yes 8408660 08/22/14 08/27/14 1 5
8408660-8LK1 8is (2-chloroisooroovll Ether 0 Yes 8408660 08/22/14 08/27/14 1 5 1
B408660-8LK1 8is (2-ethvlhexvll Phthalate 0 Yes 8408660 08/22/14 08/27/14 5 10 1
B408660-BLK1 Butvlbenzvlohthalate 0 Yes 8408660 08/22/14 08/27/14 0.6 5 1
B408660-8LK1 Carbazole 0 Yes 8408660 08/22/14 08/27/14 0.8 5 1
Page 34 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 74 of90 Ana vzed MDL MRL DF
8408660-BLK1 Chrvsene 0 Yes 8408660 08/22/14 08/27/14 2 5 1
8408660-BLK1 Dibenzo (a,hl anthracene 0 Yes 8408660 08/22/14 08/27/14 1 5 1
8408660-8LK1 Dibenzofuran 0 Yes 8408660 08/22/14 08/27/14 0.6 5 1
B408660-8LK1 Diethvlphthalate 0 Yes 8408660 08/22/14 08/27/14 0.6 5 1
8408660-8LK1 Dimethvl ohthalate 0 Yes 8408660 08/22/14 08/27/14 0.8 5 1
8408660-8LK1 Di-n-butvlohthalate 0 Yes 8408660 08/22/14 08/27/14 3 5 1
8408660-BLK1 Di-n-Octvlohthalate 0 Yes 8408660 08/22/14 08/27/14 0.5 5 1
8408660-8LK1 Diphenylamine 0 Yes 8408660 08/22/14 08/27/14 2 5 1
8408660-8LK1 Fluoranthene 0 Yes 8408660 08/22/14 08/27/14 0.6 5 1
8408660-8LK1 Fluorene 0 Yes 8408660 08/22/14 08/27/14 0. 7 5 1
8408660-8LK1 Hexachlorobenzene 0 Yes 8408660 08/22/14 08/27/14 1 5 1
B408660-8LK1 Hexachlorobutadiene 0 Yes 8408660 08/22/14 08/27/14 0.5 5
8408660-8LK1 Hexachlorocvclooentadiene 0 Yes 8408660 08/22/14 08/27/14 0.6 10 1
8408660-8LK1 Hexachloroethane 0 Yes 8408660 08/22/14 08/27/14 0.7 5 1
8408660-8LK1 lndeno (1.2.3-cdl Pvrene 0 Yes 8408660 08/22/14 08/27/14 2 5 1
8408660-8LK1 lsophorone 0 Yes 8408660 08/22/14 08/27/14 1 5 1
8408660-8LK1 Naohthalene 0 Yes 8408660 08/22/14 08/27/14 0.9 5 1
'
8408660-8LK1 Nitrobenzene 0 Yes 8408660 08/22/14 08/27/14 1 5 1
8408660-8LK1 Nitrobenzene-d5 56.0 23 130 28.0 50.0 Yes 8408660 08/22/14 08/27/14 1 .
8408660-8LK1 N-Nitrosodimethvlamine 0 Yes 8408660 08/22/14 08/27/14 0.6 10 1
8408660-BLK1 N-Nitrosodi-n-oroovlamine 0 Yes 8408660 08/22/14 08/27/14 0.8 5 1
8408660-8LK1 N-Nitrosodiohenvlamine 0 Yes 8408660 08/22/14 08/27/14 1 5 1
B408660-8LK1 Pentachlorophenol 0 Yes 8408660 08/22/14 08/27/14 4 10 1
8408660-BLK1 Phenanthrene 0 Yes 8408660 08/22/14 08/27/14 0.5 5 1
B408660-8LK1 Phenol 0 Yes 8408660 08/22/14 08/27/14 1 10 1
8408660-BLK1 Phenol-d5 30.0 5 130 30,0 100 Yes 8408660 08/22/14 08/27/14 1
Page 35 of 43
QCID Analvte % Rec RPD LCL
B408660-BLK1 Pvrene
8408660-BLK1 Pvridine
B408660-BLK1 Terphenvl-dl4 101 31
UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch
0 Yes 8408660
0 Yes 8408660
130 50.3 50.0 Yes 8408660
LCS -Method EPA 82700
Sampled Prepared PaQe 75 of90 Analyzed MDL MRL DF
08/22/14 08/27/14 0.6 5
08/22/14 08/27/14 1 5 1
08/22/14 08/27/14 1
B408660-BS1 1,2.4-Trichlorobenzene 41.2 44 142 34 83.3 Yes 8408660 08/22/14 08/27/14 1 5 1
ME-Recovery was outside ofthe lab control limits but was within Marginal Exceedance limit(± 4 stdev of mean recovery). Batch is considered to be in control based on recoveries of other analytes.
B408660-BS1 1.4-Dichlorobenzene 44.4 20 124 37 83.3 Yes 8408660 08/22/14 08/27/14 0.7 5
B408660-BS1 2.4.6-Tribromoohenol 74.7 20 130 74.7 100 Yes 8408660 08/22/14 08/27/14 1.
B408660-BS1 2,4-Dinitrotoluene 65.2 39 139 54 83.3 Yes 8408660 08/22/14 08/27/14 0.8 5
B408660-BS1 2-Chlorophenol 57.2 23 134 95 167 Yes 8408660 08/22/14 08/27/14 2 10
B408660-BS1 2-Fiuorobiohenvl 52.7 37 130 26.3 50.0 Yes 8408660 08/22/14 08/27/14 1
B408660-BS1 2-Fiuoroohenol 46.3 15 130 46.3 100 Yes 8408660 08/22/14 08/27/14 1
6408660-851 4-Chloro-3-methvlohenol 50.6 22 147 84 167 Yes 8408660 08/22/14 08/27/14 2 10 1
B408660-BS1 4-Nitroohenol 20.8 1 132 35 167 Yes 8408660 08/22/14 08/27/14 4 10 1
B408660-BS1 Acenaohthene 56.4 47 145 47 83.3 Yes B408660 08/22/14 08/27/14 2 5 1
8408660-BS1 Nitrobenzene-d5 63.3 23 130 31.7 50.0 Yes 8408660 08/22/14 08/27/14 1
B408660-BS1 N-Nitrosodi-n-proPvlamine 54.0 1 230 45 83.3 Yes 8408660 08/22/14 08/27/14 0.8 5 1
B408660-BS1 Pentachlorophenol 74.4 14 176 124 167 Yes 8408660 08/22/14 08/27/14 4 10 1
8408660-BS1 Phenol 28.8 5 112 48 167 Yes B408660 08/22/14 08/27/14 1 10 1
B408660-BS1 Phenol-d5 36.3 5 130 36.3 100 Yes B408660 08/22/14 08/27/14 1
B408660-BS1 Pvrene 80.8 33 125 67 83.3 Yes B408660 08/22/14 08/27/14 0.6 5 1
B408660-BS1 Terphenvl-dl4 92.7 31 130 46.3 50.0 Yes 8408660 08/22/14 08/27/14 1
Matrix Spike -Method EPA 82700
8408660-MS1 1,2.4-Trichlorobenzene 34.4 44 142 29 1408830-05 0 83.3 Yes 8408660 08/22/14 08/28/14 1 5
ME-Recovery was outside of the lab control limits but was within Marginal Exceedance limit (± 4 stdev of mean recovery). Batch is considered to be in control based on recoveries of other analytes.
8408660-MSl 1,4-Dichlorobenzene 38.4 20 124 32 1408830-05 0 83.3 Yes 8408660 08/22/14 08/28/14 0. 7 5 1
B408660-MS1 2.4,6-Tribromoohenol 81.3 20 130 81.3 1408830-05 100 Yes 8408660 08/22/14 08/28/14
B408660-MS1 2,4-Dinitrotoluene 75.6 39 139 63 1408830-05 0 83.3 Yes 8408660 08/22/14 08/28/14 0.8 5
Page 36 of 43
QCID Analvte
B408660-MS1 2-Chloroohenol
6408660-MSl 2-Fiuorobiohenvl
B408660-MS1 2-Fiuoroohenol
B408660-MS1 4-Chloro-3-methvlohenol
B408660-MS1 4-Nitroohenol
8408660-MS1 Acenaohthene
B408660-MS1 Nitrobenzene-d5
B408660-MS1 N-Nitrosodi-n-oroovlamine
8408660-MS1 Pentachlorophenol
8408660-MS1 Phenol
B408660-MS1 Phenol-dS
8408660-MS1 Pvrene
B408660-MS1 Terohenvl-dl4
% Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch
56.2 23 134 94 1408830-05 0 167 Yes 6408660
50.0 37 130 25.0 1408830-05 50.0 Yes 6408660
52.0 15 130 52.0 1408830-05 100 Yes 6408660
62.0 22 147 103 1408830-05 0 167 Yes 6408660
66.0 l 132 110 1408830-05 0 167 Yes 6408660
47.6 47 145 40 1408830-05 0 83,3 Yes 6408660
63.3 23 130 31.7 1408830-05 50.0 Yes 6408660
56.0 1 230 47 1408830-05 0 83.3 Yes 6408660
92.8 14 176 155 1408830-05 0 167 Yes 6408660
43.6 5 112 73 1408830-05 0 167 Yes 8408660
47.3 5 130 47.3 1408830-05 100 Yes 6408660
74.4 33 125 62 1408830-05 0 83.3 Yes 6408660
86.7 31 130 43.3 1408830-05 50.0 Yes 6408660
Matrix Spike Dup -Method EPA 82700
Sampled Prepared Paqe 76 of90 Analvzed MDL MRL OF
08/22/14 08/28/14 2 10 1
08/22/14 08/28/14 1
08/22/14 08/28/14 1
08/22/14 08/28/14 2 10 1
08/22/14 08/28/14 4 10 j
08/22/14 08/28/14 2 5 1
08/22/14 08/28/14 l
08/22/14 08/28/14 0.8 5 l
08/22/14 08/28/14 4 10 1
08/22/14 08/28/14 1 10 1
08/22/14 08/28/14 l
08/22/14 08/28/14 0.6 5 1
08/22/14 08/28/14 1
B408660-MSD1 1.2.4-Trichlorobenzene 34.8 1.16 44 142 80 29 1408830-05 0 83.3 Yes 6408660 08/22/14 08/28/14 1 5 1
ME-Recovery was outside ofthe lab control limits but was within Marginal Exceedance limit(± 4 stdev of mean recovery). Batch is considered to be in control based on recoveries of other analytes.
B408660-MSD1 1.4-Dichlorobenzene 40.8 6.06 20 124 80 34 1408830-05 0 83.3 Yes 6408660 08/22/14 08/28/14 0.7 5 1
8408660-MSD1 2.4.6-Tribromoohenol 80.3 20 130 80.3 1408830-05 100 Yes 6408660 08/22/14 08/28/14 1
8408660-MSD1 2.4-Dinitrotoluene 74.8 1.06 39 139 80 62 1408830-05 0 83.3 Yes 6408660 08/22/14 08/28/14 0.8 5 l
8408660-MSD1 2-Chloroohenol 58.0 3.15 23 134 80 97 1408830-05 0 167 Yes 8408660 08/22/14 08/28/14 2 10 1
8408660-MSD1 2-FiuorobiPhenvl 49.3 37 130 24.7 1408830-05 50.0 Yes 8408660 08/22/14 08/28/14 1
B408660-MSD1 2-Fiuoroohenol 52.3 15 130 52.3 1408830-05 100 Yes 6408660 08/22/14 08/28/14 1
B408660-MSD1 4-Chloro-3-methvlohenol 70.4 12.7 22 147 80 117 1408830-05 0 167 Yes 6408660 08/22/14 08/28/14 2 10
8408660-MSD1 4-Nitroohenol 57.8 13.2 132 80 96 1408830-05 0 167 Yes 8408660 08/22/14 08/28/14 4 10
8408660-MSD1 Acenaohthene 43.2 9.69 47 145 80 36 1408830-05 o 83.3 Yes 6408660 08/22/14 08/28/14 2 5
QM-07-The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery.
8408660-MSD1 Nitrobenzene-d5 55.3 23 130 27.7 1408830-05 50.0 Yes 6408660 08/22/14 08/28/14 1
B408660-MSD1 N-Nitrosodi-n-oroovlamine 52.4 6.64 1 230 80 44 1408830-05 0 83.3 Yes 6408660 08/22/14 08/28/14 0.8 5 1
Page 37 of 43
QCID Analvte %Rec RPD LCL UCL RPD Max Result QCSource Source Cone Spk Value Surr? Batch Sampled Prepared Pa~77of90 Ana zed MDL MRL OF
8408660-MSD1 Pentachlorophenol 92.0 0.866 14 176 80 153 1408830-05 0 167 Yes 8408660 08/22/14 08/28/14 4 10 l
8408660-MSD1 Phenol 42.4 2.79 5 112 80 71 1408830-05 0 167 Yes 8408660 08/22/14 08/28/14 1 10
B408660-MSD1 Phenol-d5 47.0 5 130 47.0 1408830-05 100 Yes 8408660 08/22/14 08/28/14
B408660-MSD1 Pvrene 77.6 4.21 33 125 80 65 1408830-05 0 83.3 Yes 8408660 08/22/14 08/28/14 0.6 5 1
B408660-MSD1 Terohenvl-dl4 89.3 31 130 44.7 1408830-05 50.0 Yes 8408660 08/22/14 08/28/14 ~
Page 38 of43
QCID Analvte % Rec RPD LCL UCL RPO Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 78 of90 Ana vzed MDL MRL OF
Blank -Method SM 2320 B
B408710-BLK1 Alkalinity-Bicarbonate (HC03) 0.0 8408710 08/27/14 08/28/14 0.2 1.0 1
B408710-BLK1 Alkalinity-Carbonate (C03) 0.0 8408710 08/27/14 08/28/14 0.2 1.0
B408710-BLK1 Alkalinity-C02 0.0 8408710 08/27/14 08/28/14 0.2 1.0
B408710-BLK1 Alkalinity-Hydroxide (OH) 0.0 8408710 08/27/14 08/28/14 0.2 1.0 1
B408710-BLK1 Alkalinity-Total (as CaC03l 0.0 8408710 08/27/14 08/28/14 0.2 1.0 1
B408710-BLK2 Alkalinity-Bicarbonate (HC03) 0.0 8408710 08/27/14 08/28/14 0.2 1.0 1
B408710-BLK2 Alkalinity-Carbonate (C03l 0.0 8408710 08/27/14 08/28/14 0.2 1.0 1
B408710-BLK2 Alkalinity-C02 0.0 8408710 08/27/14 08/28/14 0.2 1.0 1
B408710-BLK2 Alkalinity-Hydroxide (OHl 0.0 8408710 08/27/14 08/28/14 0.2 1.0
B408710-BLK2 Alkalinity-Total (as CaC03) 0.0 8408710 08/27/14 08/28/14 0.2 1.0 1
B408754-BLK1 Alkalinity-Bicarbonate (HC03) 0.0 8408754 09/02/14 09/02/14 0.2 1.0
8408754-BLKl Alkalinity-Carbonate (C03) 0.0 8408754 09/02/14 09/02/14 0.2 1.0 1
8408754-BLK1 Alkalinity-C02 0.0 8408754 09/02/14 09/02/14 0.2 1.0 1 -
B408754-BLK1 Alkalinity-Hydroxide (OH) 0.0 8408754 09/02/14 09/02/14 0.2 1.0 1
B408754-BLK1 Alkalinity-Total (as CaC03l 0.0 8408754 09/02/14 09/02/14 0.2 1.0
B408754-BLK2 Alkalinitv-Bicarbonate (HC03l 0.0 8408754 09/02/14 09/02/14 0.2 1.0 1
B408754-BLK2 Alkalinity-Carbonate (C03) 0.0 8408754 09/02/14 09/02/14 0.2 1.0 1
B408754-BLK2 Alkalinity-C02 0.0 8408754 09/02/14 09/02/14 0.2 1.0 1
B408754-BLK2 Alkalinity-Hydroxide (OH) 0.0 8408754 09/02/14 09/02/14 0.2 1.0 1
B408754-BLK2 Alkalinity-Total (as CaC03) 0.0 8408754 09/02/14 09/02/14 0.2 1.0 1
Calibration Blank-Method SM 2320 B
4H28012-CCB1 Alkalinity-Total (as CaC03) 0.0 4H28012 08/28/14 08/28/14 1
4102012-CCB1 Alkalinity-Total (as CaC03l 0.0 4102012 09/02/14 09/02/14 1
Calibration Check -Method SM 2320 B
4H28012-CCV1 Alkalinitv-Total (as CaC03) 104 90 110 2460 2360 4H28012 08/28/14 08/28/14 1
Page 39 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Sok Value Surr? Batch Sampled Preoared Pa~e 79 of90 Ana vzed MDL MRL OF
4102012-CCV1 Alkalinitv-Total (as CaC03) 100 90 110 2370 2360 4102012 09/02/14 09/02/14 1
Initial Cal Blank-Method SM 2320 B
4H28012-ICB1 Alkalinitv-Total (as CaC03l 0.0 4H28012 08/28/14 08/28/14 1
4102012-ICB1 Alkalinitv-Total (as CaC03) 0.0 4102012 09/02/14 09/02/14 1
Initial Cal Check-Method SM 2320 B
4H28012-ICV1 Alkalinitv-Total (as CaC03) 102 90 110 2400 2360 4H28012 08/28/14 08/28/14 1
4102012-ICV1 Alkalinitv-Total (as CaC03l 101 90 110 2380 2360 4102012 09/02/14 09/02/14 l
LCS -Method SM 2320 B
8408710-851 Alkalinitv-Total (as CaC03) 101 90 110 2390 2360 8408710 08/27/14 08/28/14 0.2 1.0 1
8408710-BS2 Alkalinity-Total (as CaC03) 102 90 110 2410 2360 8408710 08/27/14 08/28/14 0.2 1.0 1
8408754-851 Alkalinitv-Total (as CaC03l 100 90 110 2360 2360 8408754 09/02/14 09/02/14 0.2 1.0 1
8408754-852 Alkalinitv-Total (as CaC03) 100 90 110 2370 2360 8408754 09/02/14 09/02/14 0.2 1.0 1
Matrix Spike -Method SM 2320 B
B408710-MS1 Alkalinitv-Total (as CaC03l 102 80 120 677 ,. , .. ~·· 629 47.2 8408710 08/27/14 08/28/14 0.2 1.0 1 -
8408710-MS2 Alkalinitv-Total (as CaC03) 104 80 120 280 ~-~~.,_ .... , .. 231 47.2 8408710 08/27/14 08/28/14 0.2 1.0 1
B408754-MS1 Alkalinitv-Total (as CaC03) 80 120 0.0 J,40SS31)..{J5 0 47.2 8408754 09/02/14 09/02/14 0.2 1.0 1
QM-05-The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The analytical batch was accepted based on the acceptable data provided by the laboratory Control Sample(s) [LCS]
and/or LCS Duplicates.
B408754-MS2 Alkalinitv-Total (as CaC03) 106 80 120 122 XXXXXXX-XX 72.0 47.2 8408754 09/02/14 09/02/14 0.2 1.0 1
Matrix Spike Dup -Method SM 2320 B
B408710-MSD1 Alkalinitv-Total (as CaC03) 95.3 0.444 80 120 20 674 XXXX);XX-XX 629 47.2 8408710 08/27/14 08/28/14 0.2 1.0 1
B408710-MSD2 Alkalinitv-Total (as CaC03) 110 1.07 80 120 20 283 ,x.x\>:xx>:-A~< 231 47.2 8408710 08/27/14 08/28/14 0,2 1.0
B408754-MSD1 Alkalinitv-Total (as CaC03) 80 120 20 0.0 1408830-05 0 47.2 8408754 09/02/14 09/02/14 0.2 1.0 1
QM-05-The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The analytical batch was accepted based on the acceptable data provided by the Laboratory Control Sample(s) [LCS]
and/or LCS Duplicates,
B408754-MSD2 Alkalinitv-Total (as CaC03) 108 0.816 80 120 20 123 :\x::.'l\ \'' X~ 72.0 47.2 8408754 09/02/14 09/02/14 0.2 1.0 1
Page 40 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 80 of90 Ana vzed MDL MRL OF
Blank -Method SM 2540 C
B408640-BLK1 Total Dissolved Solids (TDSl 6 8408640 08/21/14 08/21/14 10 10 2
Duplicate -Method SM 2540 C
8408640-DUPl Total Dissolved Solids (TDSl 0.483 20 14900 XXXXXXX XX 15000 8408640 08/21/14 08/21/14 20 20 4
B408640-DUP2 Total Dissolved Solids (TDS) 6.50 20 87400 1408830-05 81900 8408640 08/21/14 08/21/14 500 500 100
Reference -Method SM 2540 C
8408640-SRMl Total Dissolved Solids ITDSl 104 90 110 208 200 8408640 08/21/14 08/21/14 10 10 2
Page 41 of 43
QCID Analvte %Ret RPD LCL UCL RPD Max Result QC Source Source Cone Spk Value Surr? Batch Sampled Prepared Pa~e 81 of90 Ana vzed MDL MRL OF
Calibration Check -Method SM 4500 H-8
4H23011-CCV1 pH 99.6 97 103 7.0 7.00 4H23011 08/23/14 08/23/14
Duplicate -Method SM 4500 H-8
8408622-DUP1 PH 0.00 3 6.4 XXXXXXX-XX 6.4 8408622 08/21/14 08/21/14 0.1 0.1 1 -
8408622-DUP2 pH 0.00 3 2.4 1408830-05 2.4 8408622 08/21/14 08/21/14 0.1 0.1 1
Initial Cal Check-Method SM 4500 H-8
4H23011-ICV1 PH 100 97 103 4.0 4.00 4H23011 08/23/14 08/23/14 1 .
4H23011-ICV2 pH 100 97 103 7.0 7.00 4H23011 08/23/14 08/23/14 -
4H23011-ICV3 pH 100 97 103 10.0 10.0 4H23011 08/23/14 08/23/14
Reference -Method SM 4500 H-8
8408622-SRM1 pH 100 95 105 7.0 7.00 8408622 08/21/14 08/21/14 0.1 0.1 1
8408622-SRM2 pH 99.4 95 105 7.0 7.00 8408622 08/21/14 08/21/14 0.1 0.1 1
Page 42 of 43
QCID Analvte % Rec RPD LCL UCL RPD Max Result QC Source Source Cone Sok Value Surr? Batch Sampled Prepared Pa~e 82 of90 Ana vzed MDL MRL DF
Calibration Blank -Method SM 4500 NH3-D
4101003-CCB1 Ammonia as N 0.1 4101003 09/01/14 09/01/14 1
4101003-CC82 Ammonia as N 0.1 4101003 09/01/14 09/01/14 1
4101003-CC83 Ammonia as N 0.09 4101003 09/01/14 09/01/14 1
4101003-CCB4 Ammonia as N 0.1 4101003 09/01/14 09/01/14
Calibration Check-Method SM 4500 NH3-D
4101003-CCV1 Ammonia as N 96.0 90 110 9.6 10.0 4101003 09/01/14 09/01/14 l
4101003-CCV2 Ammonia as N 99.0 90 110 9.9 10.0 4101003 09/01/14 09/01/14 l
4101003-CCV3 Ammonia as N 99.0 90 110 9.9 10.0 4101003 09/01/14 09/01/14 l
4101003-CCV4 Ammonia as N 97.0 90 110 9.7 10.0 4101003 09/01/14 09/01/14 1
Initial Cal Blank -Method SM 4500 NH3-D
4101003-IC81 Ammonia as N 0.09 4101003 09/01/14 09/01/14 l
Initial Cal Check-Method SM 4500 NH3-D
4101003-ICVl Ammonia as N 100 90 110 10.0 10.0 4101003 09/01/14 09/01/14 1·
LCSW-Method SM 4500 NH3-D
8409004-851 Ammonia as N 100 90 110 10.0 10.0 8409004 09/01/14 09/01/14 0.03 0.2 1
8409004-852 Ammonia as N 99.0 90 110 9.9 10.0 8409004 09/01/14 09/01/14 0.03 0.2
Matrix Spike-Method SM 4500 NH3-D
8409004-MSl Ammonia as N 99.4 80 120 5.1 >;;(XX\XX-X.X 0.1 5.00 8409004 09/01/14 09/01/14 0.03 0.2
8409004-MS2 Ammonia as N 96.9 80 120 5340 1408830-05 2920 2500 8409004 09/01/14 09/01/14 0.03 0.2 1
Matrix Spike Dup-Method SM 4500 NH3-D
8409004-MSD1 Ammonia as N 103 3.85 80 120 20 5.3 XXXXXXX-XX 0.1 5.00 8409004 09/01/14 09/01/14 0.03 0.2 1
8409004-MSD2 Ammonia as N 98.6 0.802 80 120 20 5380 1408830-05 2920 2500 8409004 09/01/14 09/01/14 0.03 0.2 1
PBW -Method SM 4500 NH3-D
B409004-8LK1 Ammonia as N 0.09 8409004 09/01/14 09/01/14 0.03 0.2 1
8409004-8LK2 Ammonia as N 0.1 8409004 09/01/14 09/01/14 0.03 0.2 1
Page 43 of 43
Page 83 of90
Surrogate Summary for Sample Delivery Group -1408830
QC ID Surro~ate % Rec LCL UCL -------------------------------------------
1408830-01
1408830-01
1408830-01
1408830-02
1408830-02
1408830-02
1408830-03
1408830-03
1408830-03
1408830-04
1408830-04
1408830-04
1408830-05
1408830-05
1408830-05
1408830-06
1408830-06
1408830-06
1408830-07
1408830-07
1408830-07
1408830-08
1408830-08
1408830-08
1408830-09
1408830-09
1408830-09
8408858-BLKl
8408858-8LK1
8408858-8LK1
8408858-BS1
8408858-851
Page 1 of 5
1.2-Dichloroethane-d4
4-Bromofluorobenzene
Toluene-d8
1.2-Dichloroethane-d4
4-8romofluorobenzene
Toluene-d8
1.2-Dichloroethane-d4
4-8romofluorobenzene
Toluene-dB
1,2-Dichloroethane-d4
4-8romofluorobenzene
Toluene-d8
1,2-Dichloroethane-d4
4-8romofluorobenzene
Toluene-dB
1.2-Dichloroethane-d4
4-8romofluorobenzene
Toluene-dB
1,2-Dichloroethane-d4
4-8romofluorobenzene
Toluene-dB
1.2-Dichloroethane-d4
4-8romofluorobenzene
Toluene-dB
1,2-Dichloroethane-d4
4-8romofluorobenzene
Toluene-d8
1.2-Dichloroethane-d4
4-8romofluorobenzene
Toluene-d8
1.2-Dichloroethane-d4
4-8romofluorobenzene
Method EPA 82608
127
108
103
125
109
102
120
108
101
119
109
102
122
111
103
127
110
102
124
111
101
126
111
103
113
108
103
109
106
101
106
105
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
Result Sok Value Batch DF ------
63.4
54.2
51.6
62.3
54 4
51.2
60.0
54.0
50.6
59.5
54.6
51.0
61.0
55.4
51.4
63.4
54.8
50.8
62.0
55.7
50.3
62.8
55,4
51.4
11.3
10.8
10.3
10.9
10,6
10.1
10.6
10.5
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408909
8408858
8408858
8408858
8408858
8408858
8408858
8408858
8408858
1
1
1
1
1
1
l
1
l
l
l
1
1
1
1
1
1
1
1
1
1
1
Page 84 of90
QCID Surrogate % Rec LCL UCL Result Spk Value Batch OF
8408858-851 Toluene-d8 101 70 130 10.1 10.0 8408858 1
8408858-MS1 1,2-Dichloroethane-d4 103 70 130 51.4 50.0 8408858 1
8408858-MS1 4-8romofluorobenzene 103 70 130 51.7 50.0 8408858 1
8408858-MS1 Toluene-d8 101 70 130 50.4 50.0 8408858 1
8408858-MSD1 1.2-Dichloroethane-d4 106 70 130 53.0 50.0 8408858 1
8408858-MSD1 4-8romofluorobenzene 105 70 130 52.4 50.0 8408858 1
8408858-MSD1 Toluene-d8 102 70 130 50.8 50.0 8408858 1
8408909-BLK1 1,2-Dichloroethane-d4 110 70 130 11.0 10.0 8408909 1
8408909-8LK1 4-8romofluorobenzene 108 70 130 10.8 10.0 8408909 1
8408909-8LK1 Toluene-d8 102 70 130 10.2 10.0 8408909 1
8408909-851 1.2-Dichloroethane-d4 110 70 130 11.0 10.0 8408909 1
8408909-951 4-8romofluorobenzene 105 70 130 10.5 10.0 8408909 1
8408909-851 Toluene-d8 102 70 130 10.2 10.0 8408909 1
8408909-MS1 1.2-Dichloroethane-d4 120 70 130 59.8 50.0 8408909 1
8408909-MS1 4-8romofluorobenzene 107 70 130 53.4 50.0 8408909 1
8408909-MS1 Toluene-d8 102 70 130 51.1 50.0 8408909 1
8408909-MS2 1.2-Dichloroethane-d4 106 70 130 53.2 50.0 8408909
8408909-MS2 4-8romofluorobenzene 106 70 130 53.1 50.0 8408909 1
8408909-MS2 Toluene-d8 102 70 130 50.8 50.0 8408909 1
8408909-MSD1 1.2-Dichloroethane-d4 120 70 130 60.0 50.0 8408909 1
8408909-MSD1 4-8romofluorobenzene 106 70 130 53,2 50.0 8408909 1
8408909-MSD1 Toluene-dB 102 70 130 50.8 50.0 8408909 1
Page2of5
Page 85 of90
_ _:O:..:C:...:I.:.D ______ s:..:u:...:r..:ro:..:g::a.:.te:.._ _________ ~%:...:R.:.e:...:c__:l:..:C.:.l _ __.:.u.:.c:.l ________ R.:.e:..:s..:.:.ult Spk Value Batch DF
Method EPA 82700
1408830-01 2.4.6-Tribromoohenol 96 7 20 130 96.7 100 8408660 1
1408830-01 2-Fiuorobiohenvl 62.0 37 130 31.0 50.0 8408660 1
1408830-01 2-Fiuoroohenol 67.7 15 130 67.7 100 8408660 1
1408830-01 Nitrobenzene-d5 86.7 23 130 43.3 50.0 8408660 1
1408830-01 Phenol-d5 75.7 5 130 75.7 100 8408660
1408830-01 Terohenvl-dl4 91,3 31 130 45.7 50.0 8408660 1
1408830-02 2.4,6-Tribromoohenol 98.0 20 130 98.0 100 8408660 1
1408830-02 2-Fiuorobiohenvl 62.0 37 130 31.0 50.0 8408660 1
1408830-02 2-Fiuoroohenol 70.0 15 130 70.0 100 8408660
1408830-02 Nitrobenzene-d5 80.0 23 130 40.0 50.0 8408660 1
1408830-02 Phenol-d5 67.7 5 130 67.7 100 8408660
1408830-02 Terohenvl-dl4 95.3 31 130 47.7 50.0 8408660
1408830-03 2.4.6-Tribromoohenol 83.7 20 130 83.7 100 8408660
1408830-03 2-Fiuorobiohenvl 60.0 37 130 30.0 50,0 8408660
1408830-03 2-Fiuoroohenol 69.3 15 130 69.3 100 8408660
1408830-03 Nitrobenzene-d5 72.0 23 130 36.0 50,0 8408660 1
1408830-03 Phenol-d5 58,3 5 130 58.3 100 8408660
1408830-03 Terohenvl-dl4 98.0 31 130 49.0 50,0 8408660 1
1408830-04 2.4,6-Tribromophenol 93,7 20 130 93.7 100 8408660 1
1408830-04 2-Fiuorobiohenvl 60.7 37 130 30.3 50.0 8408660 1
1408830-04 2-Fiuoroohenol 62_3 15 130 62.3 100 8408660 1
1408830-04 Nitrobenzene-d5 79.3 23 130 39.7 50.0 8408660 1
1408830-04 Phenol-d5 56.7 5 130 56.7 100 8408660 1
1408830-04 Terphenvl-dl4 90.7 31 130 45.3 50.0 8408660 1
1408830-05 2.4.6-Tribromoohenol 82.3 20 130 82.3 100 8408660
1408830-05 2-Fiuorobiohenvl 52.0 37 130 26.0 50.0 8408660 1
1408830-05 2-Fiuoroohenol 55.0 15 130 55.0 100 8408660 1
1408830-05 Nitrobenzene-d5 64.7 23 130 32.3 50.0 8408660
1408830-05 Phenol-d5 48.0 5 130 48.0 100 8408660 1
1408830-05 Terohenvl-dl4 95.3 31 130 47.7 50.0 8408660 1
1408830-06 2.4,6-Tribromoohenol 93.7 20 130 93.7 100 8408660 1
1408830-06 2-Fiuorobiohenvl 62.0 37 130 31.0 50.0 8408660 1
1408830-06 2-Fiuoroohenol 63.3 15 130 63.3 100 8408660 1
1408830-06 Nitrobenzene-d5 72.7 23 130 36.3 50.0 8408660 1
Page 3 of 5
Page 86 of90
QCID Surrogate % Rec LCL UCL Result Spk Value Batch DF
1408830-06 Phenol-d5 65.7 5 130 65.7 100 8408660
1408830-06 Terohenvl-dl4 993 31 130 49.7 50.0 8408660 1
1408830-07 2.4,6-Tribromoohenol 95.0 20 130 95.0 100 8408660 l
1408830-07 2-Fiuorobiphenvl 62.7 37 130 31.3 50.0 8408660 l
1408830-07 2-Fiuorophenol 63.7 15 130 63.7 100 8408660 l.
1408830-07 Nitrobenzene-d5 78.7 23 130 39.3 50.0 8408660
1408830-07 Phenol-d5 68.0 5 130 68.0 100 8408660 1
1408830-07 Terphenvl-dl4 100 31 130 50.0 50.0 8408660 1
1408830-08 2.4.6-Tribromophenol 94.0 20 130 94.0 100 8408660 1
1408830-08 2-Fiuorobiphenvl 72.7 37 130 36.3 50.0 8408660 1
1408830-08 2-Fiuorophenol 66.7 15 130 66.7 100 8408660
1408830-08 Nitrobenzene-d5 80.0 23 130 40.0 50.0 8408660
1408830-08 Phenol-d5 63.0 5 130 63.0 100 8408660
1408830-08 Terphenvl-dl4 97.3 31 130 48.7 50.0 8408660 1
8408660-8LK1 2.4.6-T ribro mop he no I 58.0 20 130 58.0 100 B408660 l
8408660-8LK1 2-Fiuorobiphenvl 52.0 37 130 26.0 50.0 8408660 1
8408660-8LK1 2-Fiuorophenol 48.0 15 130 48 0 100 B408660 1
8408660-8LK1 Nitrobenzene-d5 56.0 23 130 28.0 50.0 8408660 1
8408660-8LK1 Phenol-d5 30.0 5 130 30.0 100 8408660 1
8408660-8LK1 Terphenvl-dl4 101 31 130 50.3 50.0 8408660 1
8408660-851 2.4.6-Tribromophenol 74.7 20 130 74.7 100 8408660 1
8408660-851 2-Fiuorobiphenvl 52.7 37 130 26.3 50.0 8408660 1
8408660-851 2-Fiuorophenol 46.3 15 130 46.3 100 8408660
8408660-851 Nitrobenzene-d5 63.3 23 130 31.7 50.0 8408660 1
8408660-851 Phenol-d5 36,3 5 130 36.3 100 8408660 1
8408660-851 Terphenvl-dl4 92.7 31 130 46.3 50.0 8408660 1
8408660-MS1 2.4,6-Tribromophenol 81.3 20 130 81.3 100 8408660 1
8408660-M$1 2-Fiuorobiphenvl 50.0 37 130 25.0 50.0 8408660 1
8408660-MS1 2-Fiuorophenol 52.0 15 130 52.0 100 8408660 1
8408660-MS1 Nitrobenzene-d5 63.3 23 130 31.7 50.0 8408660 1
8408660-MS1 Phenol-d5 47.3 5 130 47.3 100 8408660 1
8408660-M$1 Terphenvl-dl4 86.7 31 130 43.3 50.0 8408660 1
8408660-MSD1 2.4,6-Tribromoohenol 80.3 20 130 80.3 100 8408660 1
8408660-MSD1 2-Fiuorobiphenvl 49.3 37 130 24.7 50.0 8408660 1
8408660-MSD1 2-Fiuorophenol 52.3 15 130 52.3 100 8408660 1
Page 4 of 5
Page 87 of90
QCID Surrol!ate % Rec LCL UCL Result Spk Value Batch DF
B408660-MSD1 Nitrobenzene-d5 55.3 23 130 27.7 50.0 8408660 1
B408660-MSD1 Phenol-dS 47.0 5 130 47 0 100 8408660 1
B408660-MSD1 Terphenvl-dl4 89.3 31 130 44.7 50.0 8408660 1
Page 5 of 5
Page 88 of90
I
CHEMTECH -FORD ANAL YTJCAL LABORATORY CHAIN OF CUSTODY
Jan Dalla
COMPANY: Ene<JV Fuels Resources (USA) Inc. BIWNG ADDRESS: US Unoon Boulevard. Sui!@ 600
ADORESS: 6425 South Highway 191 BIWNG CITY/STATE/ZIP: Lakewood. Colorado 80228
OTY/STATE/ZIP: Blandin![ Utah 845U PURCHASIO ORDER 1:
PHON£8: 435-678·4115 FAll: CHEMTECH-FORD
LA9()PATQil 1 ~"--
Wh1re M~a M1ll ·"' ~.) Garnn Palmer PROJECT: CONTACT:
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Delivery Method:
::; UPS ~: USPS
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~Walk-in _·Courier
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CHEMTECH FORD LABORATORIES
Sample Receipt
R . . T · I j ·c ece1vmg emperature 1
i~ 1:~~-?~A· .. I \ r 1''1 ·-:l,!J • ;j'_ ,L '~~: -;)._·. ... ~ ...
Comments
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[ ~2:. .'.~2·~::.::-~
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1""<19" Ol1 01 ::IV
Certificate of Analysis
CHEMTECH-FORD
LABORATORIES
Report Footnotes
Abbreviations
ND =Not detected at the correeponding Minimum Reporting Limit.
I mg/L =one milligram per liter or I m&'J(g-one milligram per kilogram= 1 part per million.
I ugiL = one microgram per liter or I u&'J(g = one microgram per kilogram = I part per billion.
1 ng/L = one nanogram per liter or I ng/Kg = one nanogram per kilogram= I part per trillion.
Flaa Descriptions
SPH = Sample submitted past method specified holding time.
www.chemlechford.com
MainReport-no SUIT rpt
Page 90 of90
9632 South 500 West
Sandy, UT 84070
801-262-7299 Office
t!;lijll l Laboratories LLc
a member of The GEL Group INC PO Box 30712 Charleston, SC 29417
2040 Savage Road Charleston, SC 29407
P 843.556.8171 F 843.766.1178
October 14,2014
Ms. Kathy Weinel
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Re: White Mesa Mill GW
Work Order: 358469
Dear Ms. Weinel:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on August 25, 2014. This original data report has been prepared and reviewed in
accordance with GEL's standard operating procedures.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 4487.
Purchase Order: DW16138
Enclosures
p.J 1~111111
Sincerely,
Sylainna Rivers
Project Manager
www.gel.com
Page 2 of21
Energy Fuels Resources (USA), Inc.
White Mesa Mill GW
SDG: 358469
Page 3 of21
October 14, 2014
Laboratory Identification:
GEL Laboratories LLC
2040 Savage Road
Charleston, South Carolina 29407
[phone]
Summary:
Receipt Narrative
for
Energy Fuels Resources (USA), Inc.
SDG: 358469
Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on August 25, 2014
for analysis. Chain of custody needed clarification on laboratory filtration request. Analysis was performed on
lab filtration under workorder 358469. All sample containers arrived without any visible signs of tampering or
breakage. There are no additional comments concerning sample receipt.
Sample Identification: The laboratory received the following samples:
Case Narrative:
Laboratory ID
358469001
358469002
358469003
358469004
358469005
358469006
358469007
358469008
Client ID
Celli
Cell 2 Slimes
Cell3
Cell4A
Cell4A LDS
Cell4B
Cell4B LDS
Cell65
Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any
technical or administrative problems during analysis, data review, and reduction are contained in the analytical
case narratives in the enclosed data package.
The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt
Checklist, Data Package Qualifier Definitions and data from the following fractions : Radiochemistry.
Sylainna Rivers
Project Manager
Page 4 of21
Samples Shipped to:
Pro oct
Sam le 10
Cell1
Cell 2 snmes
Cell3
Caii4A
Cell 4A LOS
Cell 4B
Ceii4B LOS
Cell65
Comments:
Relinquish ad BY:( Signature)
Tanner Holliday
Re\lnQulshcd By:(~igrmturo)
:
CHAIN OF CUSTODY
..,:;G;:;e-:-:1 L="a="b.;;..or;.;;;a;.;.;lo"'ri:-cso......,:-------Contact:
2040 Savage Road
Charleslon, SC 29407
Sam tors Name
Tlme
Date Collected Collected
Bf19f2D14 815
8(19/2014 825
6(19/2014 900
ll/19/201 •1 925
8/19/2014 940
8/19/2014 10f0
8(19/2014
Datemme Received By:(Signature)
Dalerrtme
Datemma
ln Daily check performed and passed on
IR tcmpemL.urc gun?
3 Chain of custody documents included
wilh shipment?
4 Sample containers intact and scaled?
5 Samples requiring chcmicnl
preservation at proper pH?
6 VOA vials free of head space (defined
as < 6mm bubble)'?
received within holding
!D's on COC match !D's on
10 Date & Lime on COC malch dntc &
time on bottles'/
11 Nmnbcr of containers received match
number indicated on COC?
Arc sample containers idcnti fiablc ns
provided'/
and !racking number.
(U.Ie
Page 5 of21
Leaking .contulncr Olhcr (de>cribe)
ice Dry icc None Other (dc.<cribe)
•ulltcmpcrnlllrcs nrc recorded In Cel~lus
~ I Tcmpcr•ture Device Serial// (If Applic~hlc): \
Circle Applicable:
Seal~ broken Damngcd container Leaking (Oillaincr Other (describe)
Sumple ID's, (Ontulnc~ uftcctcd und observed pH:
Circle Applicable:
FedEx Air Fed Ex Orounu UPS Field Services Courier Olhcr
1'2-
GEL Laboratories LLC -Login Review Report
GEL Work Order/SDG: 358469
Client SDG: 358469
Relog of 355403001
Project Manager:
Project Name:
Purchase Order:
Package Level:
EDD Format:
Sylainna Rivers
DNMI00100 White Mesa Mill GW
DW16138
LEVEL3
EIM_DNMI
GELID Client Sample ID Client Sample Desc.
358469001 Cell1 -Relog from 355403001
358469002 Cell2 Slimes -Relog from 355403002
358469003 Cell3 -Relog from 355403003
358469004 Ceii4A -Relog from 355403004
358469005 Cell 4A LOS -Relog from 355403005
358469006 Ceii4B -Relog from 355403006
358469007 Ceii4B LOS -Relog from 355403007
358469008 Cell65 -Relog from 355403008
Client Sample ID Status Tests/Methods
-001 Cell1 NEW GFPC, Total Alpha Radium,
Liquid
NEW Laboratory Composite-FILTER
-002 Cell 2 Slimes NEW GFPC, Total Alpha Radium,
Liquid
NEW Laboratory Composite-FILTER
-003 Cell3 NEW GFPC, Total Alpha Radium,
Liquid
NEW Laboratory Composite-FILTER
-004 Ceii4A NEW GFPC, Total Alpha Radium,
Liquid
NEW Laboratory Composite -FILTER
-005 Cell 4A LOS NEW GFPC, Total Alpha Radium,
Liquid
NEW Laboratory Composite -FILTER
-006 Ceii4B NEW GFPC, Total Alpha Radium,
Liquid
NEW Laboratory Composite-FILTER
-007 Cell 4B LOS NEW GFPC, Total Alpha Radium,
Liquid
NEW Laboratory Composite-FILTER
-008 Cell65 NEW GFPC, Total Alpha Radium,
Liquid
NEW Laboratory Composite -FILTER
Collect
Date & Time
19-AUG-14 08:15
19-AUG-14 08:25
19-AUG-14 09:00
19-AUG-14 09:25
19-AUG-14 09:40
19-AUG-14 10:10
19-AUG-14 10:00
19-AUG-14 09:40
Product
Reference
Gross Alpha
LAB FILTER
Gross Alpha
LAB FILTER
Gross Alpha
LAB FILTER
Gross Alpha
LAB FILTER
Gross Alpha
LAB FILTER
Gross Alpha
LAB FILTER
Gross Alpha
LAB FILTER
Gross Alpha
LAB FILTER
Work Order Due Date: 15-0CT-14
Package Due Date:
EDD Due Date:
Due Date:
14-0CT-14
15-0CT-14
15-0CT-14
GL Review Fractions: Rad
Receive Time #of Lab
Date & Time Zone Cont. Matrix
25-AUG-14 09:00 -2 1 GROUND WATER
25-AUG-14 09:00 -2 1 GROUND WATER
25-AUG-14 09:00 -2 1 GROUND WATER
25-AUG-14 09:00 -2 1 GROUND WATER
25-AUG-14 09:00 -2 1 GROUND WATER
25-AUG-14 09:00 -2 1 GROUND WATER
25-AUG-14 09:00 -2 1 GROUND WATER
25-AUG-14 09:00 -2 1 GROUND WATER
Fax Date PM Comments
Relog of 355403001
Relog of 355403002
Relog of 355403003
Relog of 355403004
Relog of 355403005
Relog of 355403006
Relog of 355403007
Relog of 355403008
Report Date: 14-0CT -14
Work Order: 358469
Page 1 of 2
Collector: C
Prelogin #: 20140820530
Project Workdef ID: 1294356
SDG Status: Closed
Logged by: HX51
Fax Days to Prelog Lab Field
Due Date Process CofC# Group QC QC
15-0CT-14 20
15-0CT-14 20
15-0CT-14 20
15-0CT-14 20
15-0CT-14 20
15-0CT-14 20
15-0CT-14 20
15-0CT-14 20
Receive
Aux Data Codes
,......,
N
4-< 0
\0
Q)
~ 0...
GEL Laboratories LLC -Login Review Report
Product: LABCOMP _L Workdef ID: 1295580
Method:
Product Description: Laboratory Composite -FILTER
Samples: 001, 002, 003, 004, 005, 006, 007, 008
Parmname Check: All parmnames scheduled properly
CAS# Parmname
Product: GFCTORAL Workdef ID: 1297250
Method: EPA 900.1 Modified
Product Description: GFPC, Total Alpha Radium, Liquid
Samples: 001,002,003,004,005,006,007,008
Parmname Check: All parmnames scheduled properly
CAS# Parmname
Gross Radium Alpha
In Product Group? No
In Product Group? No
Action Product Name Description
Contingent
Tests
Login Requirements:
Requirement
Group Name:
Client RDL or
PQL & Unit
Group Name:
Client RDL or
PQL & Unit
Samples
Reporting
Units
Reporting
Units
pCi!L
Include? Comments
Peer Review by: ____________ _ Work Order (SDG#), PO# Checked? ____ _
Group Reference:
Path: Standard
Report Date: 14-0CT -14
Work Order: 358469
Page 2 of 2
Product Reference: LAB FILTER
Moisture Correction: "As Received"
Parm Included Included Custom
Function in Sample? in QC? List?
Group Reference:
No
Path: Standard
Product Reference: Gross Alpha
Moisture Correction: "As Received"
Parm Included Included Custom
Function in Sample? in QC? List?
REG y y Yes
C of C signed in receiver location? _____ _
-N ........ 0
r-
(!)
01) ro A-.
Page 9 of21
Method/ Analysis Information
Radiochemistry Case Narrative
Energy Fuels Resources (DNMI)
SDG 358469
Product: GFPC, Total Alpha Radium, Liquid
Analytical Method: EPA 900.1 Modified
Analytical Batch Number: 1426429
Sample ID
358469001
358469002
358469003
358469004
358469005
358469006
358469007
358469008
1203185350
1203185354
1203185351
1203185352
1203185353
Client ID
Cell 1
Cell 2 Slimes
Cell3
Cell4A
Cell4ALDS
Cell4B
Cell4B LDS
Cell65
MB for batch 1426429
Laboratory Control Sample (LCS)
358469001(Cell1) Sample Duplicate (DUP)
358469001(Cell 1) Matrix Spike (MS)
358469001(Cell1) Matrix Spike Duplicate (MSD)
The samples in this SDG were analyzed on an "as received" basis.
SOP Reference
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with
GL-RAD-A-010 REV# 15.
Calibration Information:
Calibration Information
All initial and continuing calibration requirements have been met.
Standards Information
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
before the expiration dates.
Sample Geometry
All counting sources were prepared in the same geometry as the calibration standards.
Page 10 of21
Quality Control (OC) Information:
Blank Information
The blank volume is representative of the sample volume in this batch.
Designated QC
The following sample was used for QC: 358469001 (Cell 1).
QC Information
All of the QC samples meet the required acceptance limits with the following exceptions: The blank,
1203185350 (MB), did not meet the detection limit due to keeping the blank volume consistent with the other
sample aliquots. All other samples met the detection limits. The matrix spike and matrix spike duplicate,
1203185352 (Cell 1) and 1203185353 (Cell I), did not meet recovery requirements due to the sample activity
being greater than five times the spiked nominal concentration.
Technical Information:
Holding Time
All sample procedures for this sample set were performed within the required holding time.
Sample Re-prep/Re-analysis
None of the samples in this sample set required reprep or reanalysis.
Chemical Recoveries
All chemical recoveries meet the required acceptance limits for this sample set.
Recounts
Sample 358469008 (Cell 65) was recounted to verify sample result. The second count is reported.
Miscellaneous Information:
Data Exception (DER) Documentation
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
SOP or contractual documents. A data exception report (DER) was not generated for this SDG.
Sample-Specific MDA/MDC
The MD A/MDC reported on the certificate of analysis is a sample-specific MDNMDC.
Additional Comments
Samples were filtered per lab comp instructions and reanalyzed for Total Alpha Radium. Reporting results.
Qualifier Information
Manual qualifiers were not required.
Certification Statement
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 11 of21
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Qualifier Definition Report
for
DNMIOOl Energy Fuels Resources (USA), Inc.
Client SDG: 358469 GEL Work Order: 358469
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a surrogate compound
U Analyte was analyzed for, but not detected above the CRDL.
Review/Validation
GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables
receive a third level review of the fractional data package.
The following data validator verified the information presented in this data report:
Signature: 9l 0 G...J1_u ~ · 1'-t <... ( (...f (I {j
Date: 14 OCT 2014
Name: Heather McCarty
Title: Analyst II
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407-[phone] -www.gel.com
QC Summary
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Contact:
Workorder:
Parmname
Rad Gas Flow
Suite 600
Lakewood, Colorado
Ms. Kathy Weinel
358469
Batch 1426429
QC1203185351 358469001 DUP
Gross Radium Alpha
QC1203185354 LCS
Gross Radium Alpha
QC1203185350 MB
Gross Radium Alpha
QC1203185352 358469001 MS
Gross Radium Alpha
QC1203185353 358469001 MSD
Gross Radium Alpha
Notes:
NOM
Uncertainty
5500
Uncertainty
Uncertainty
5660
Uncertainty
5660
Uncertainty
Sample Qual
3.31E+05
+/-710
u
3.31E+05
+/-710
3.31E+05
+/-710
Counting Uncertainty is calculated at the 68% confidence level (!-sigma).
The Qualifiers in this report are defined as follows:
**
<
>
Analyte is a surrogate compound
Result is less than value reported
Result is greater than value reported
The TIC is a suspected aldol-condensation product
QC Units
3.75E+05 pCi!L
+/-707
4970 pCi/L
+/-84.9
-0.45 pCi!L
+/-4.99
3.10E+05 pCi/L
+/-651
3.20E+05 pCi/L
+/-670
RPD%
12.3
3.36
A
B
BD
c
D
F
H
K
L
M
M
For General Chemistry and Organic analysis the target analyte was detected in the associated blank.
Results are either below the MDC or tracer recovery is low
Analyte has been confirmed by GC/MS analysis
Results are reported from a diluted aliquot of the sample
Estimated Value
Analytical holding time was exceeded
Analyte present. Reported value may be biased high. Actual value is expected to be lower.
Analyte present. Reported value may be biased low. Actual value is expected to be higher.
M if above MDC and less than LLD
Matrix Related Failure
N/A RPD or %Recovery limits do not apply.
Nl See case narrative
ND Analyte concentration is not detected above the detection limit
Page 20 of21
Reuort Date: October 14, 2014
Page 1 of 2
REC% _B_an e Anlst Date Time
(0%-20%) CXP3 10/13/14 15:38
90.3 (75%-125%) 10/13/14 16:31
10/13/14 15:37
N/A (75%-125%) 10/13/14 15:37
N/A (0%-20%) 10/13/14 16:32
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407-[phone]-www.gel.com
QC Summary
Workorder: 358469
Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst
NJ
Q
R
u
UI
UJ
UL
X
y
1\
h
Consult Case Narrative, Data Summary package, or Project Manager conceming this qualifier
One or more quality control criteria have not been met. Refer to the applicable narrative orDER.
Sample results are rejected
Analyte was analyzed for, but not detected above the CRDL.
Gamma Spectroscopy--Uncertain identification
Gamma Spectroscopy--Uncertain identification
Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
Consult Case Narrative, Data Summary package, or Project Manager conceming this qualifier
QC Samples were not spiked with this compound
RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
Preparation or preservation holding time was exceeded
Page 2 of 2
Date Time
N/ A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable.
"The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/-the
RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
Page 21 of21
TabD
Chemical and Radiological Summary Tables
Celll
Chemical and Radiolocical Characteristics
Constituent 1987 2003 2007 2008 2009 2010 2011 2012 2013 2013 2014 (Avg) (Avg) (resam}!le)
Major Ions (JD2/I)
Carbonate <5 <1 ND ND <I <1 <1 <1 <I NS <1
Bicarbonate <5 NA ND ND <1 <1 <1 <1 <1 NS <1
Calcium 630 307 483.8 604 635 711 577 426 768 NS 404
Chloride 8000 6728 37340 9830 20700 7440 33800 78000 9900 NS 11600
Fluoride <100 3005 31.72 0.3 0.4 28.4 69.2 62.9 4130 _NS 2380
Magnesium 7900 5988 21220 6550 16200 5410 14300 16000 4470 NS 5530
Nitrogen-Ammonia 7800 3353 10628 5250 15200 8120 12900 9750 3900 NS 5700
Nitrogen-Nitrate <100 41.8 269.4 64.9 142 58 212 556 128 NS 53.0
Potassium NA 647 5698 1880 4140 1840 4510 9750 6580 NS 3010
Sodium 10000 8638 62600 13200 39000 16700 29500 41700 15900 NS 12200
Sulfate 190000 63667 287600 118000 232000 107000 182000 158000 100000 NS 124000
pH (s.u.) 0.70 1.88 0.80 1.53 1.15 2.73 2.23 1.9 2.74 NS 1.3
TDS 120000 94700 357400 131000 140000 130000 216000 342000 149000 NS 159000
Conductivity (urnhos/cm) NA NA NA NA 365000 110000 112000 136000 94200 NS 113000
Metals (U211)
Arsenic 440000 121267 849000 271000 436000 74400 299000 25500 9800 NS 249000
Beryllium 780 475 2262 500 410 338 1270 3180 415 NS 448
Cadmium 6600 3990 29320 8790 9120 2940 13700 30700 2380 NS 3060
Chromium 13000 6365 29940 6760 18700 5620 22700 12100 8350 NS 13200
Cobalt 120000 NA 88240 23500 97500 16200 56000 53100 25500 NS 56500
Copper 740000 196667 881000 360000 168000 125000 483000 885000 544000 NS 3420000
Iron 3400000 2820000 13480000 3280000 2390000 3400000 8940000 840000 1420000 NS 2520000
Lead <20000 3393 27420 11200 10600 9240 23600 17000 2810 NS 13500
Manganese 140000 162500 990200 206000 723000 173000 735000 1560000 188000 NS 162000
Mercury NA NA ND ND 7.61 7.2 61.4 117 6.16 NS 12.5
Molybdenum 240000 50550 415600 106000 142000 35300 235000 434000 16800 NS 68800
Nickel 370000 36950 40860 32000 156000 27500 43700 15000 39100 NS 129000
Selenium <20000 1862 15420 13000 14800 5220 11600 8090 2690 NS 3970
Silver <5000 NA 1559.2 449 558 155 1110 4310 329 NS 336
Thallium 45000 NA 407.8 165 387 193 560 13 63.3 NS 876
Tin <5000 NA 6512 1240 2290 263 1500 <100 <100 NS <17000
Uranium 105000 134517 788600 416000 578000 159000 838000 1450000 140000 NS 137000
Vanadium 280000 348000 2208200 1200000 773000 752000 2500000 1940000 98200 NS 485000
Zinc 1300000 NA 642940 476000 229000 171000 398000 811000 228000 NS 229000
Radiologies (pCi/1)
Gross Alpha NA 169333 1 29380 21900 16500 11300 3610 12600 32700 NS 331000
VOCS(ug/L)
Acetone 35 NA 66.5 110 710 260 80 310 41.1 NS <700
Benzene <5 NA ND ND <I <I <1 <1 <I NS <5.0
Carbon tetrachloride <5 NA ND ND <1 <1 <1 <1 <I NS <5.0
Chloroform 8 NA 6.7 6.6 16 4.9 13 19 7.62 NS <70.0
Chloromethane NA NA ND 9.4 11 4.4 3.6 4.0 5 NS <30.0
Celll
Ch I and Radiolo!!ical Ch 3 terisf
Constituent 1987 2003 2007 2008 2009 2010 2011 2012 2013 2013 2014 (AvJD (AvJD (resample)
MaJor Ions (mWl)
MEK NA NA ND ND 120 65 <1 200 <20 NS <4000
Methylene Chloride 11 NA ND ND 2.0 <1 <1 2 <1 NS <5.0
Naphthalene <10000 NA <10 ND 1.1 5.4 2 3 <1 NS <100
Tetrahvdrofuran NA NA 150 <20 <100 <10 <500 2.9 <I NS <46.0
Toluene <5 NA ND ND <1 <1 <1 <1 <1 NS <1000
Xylenes <5 NA ND ND <1 <1 <1 <1 <I NS <10000
SVOCS (ug/L) - -
1.2,4-Trichlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
1,2-Dichlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
1 ,3-Dichlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
1,4-Dichlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
l•Methylnaphthl.).leoe NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
2,4,5-Trichlorophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
2,4,6-Trichlorophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
2.4-Dichloro_phenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
2,4-Dimethylpheno1 NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
2,4-Dinitrophenol NA NA NA NA <250 <20 <20 <20 <21.6 <20 <20
2,4-Dinitrotoluene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
2,6-Dinitrotoluene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
2-Chloronaphthalene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
2-Chlorophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
2-Methvlnaphthalene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
2-Methylphenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
2-Nitrophenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
3&4-Methvlphenol NA NA NA NA <22 <10 <10 <10 <10.8 <10 <10
3,3 '-Dichlorobenzidine NA NA NA NA <100 <10 <10 <10 <10.8 <10 <10
4,6-Dinitro-2-methylphenol NA NA NA NA <250 <10 <10 <10 <10.8 <10 <10
4-Bromophenyl phenyl ether NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
4-Chloro-3-methyl phenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
4-Chlorophenvl phenyl ether NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
4-Nitrophenol NA NA NA NA <250 <10 <10 <10 <10.8 <10 <10 I
Acenaphthene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Acenaphthvlene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Anthracene NA NA NA NA <50 <10 <10 <LO <10.8 <10 <10 i
Azobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 I
Benz(a)anthracene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Benzidine NA NA NA NA <100 <10 <10 <10 <10.8 <10 41
Benzo(a)pyrene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Benzo(b )fluoranthene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Benzo(g.h,i)pervlene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Benzo(k)fluoranthene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Bis(2-chloroethoxy)methane NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 I
Bis(2-chloroethvl) ether NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Bis(2-chloroisopropy1) ether NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Celll
Ch I and Radioloeical Ch terisf
Constituent 1987 2003 2007 2008 2009 2010 2011 2012 2013 2013 2014 I (Av2) (Av2) (resample)
Maior Ions (mg/1) I
Bis(2-ethylhexyl) phthalate NA NA NA NA <50 27 <10 <10 <10.8 <10 <10 I
Butyl benzyl phthalate NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 I
Chrysene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10 I
Dibenz(a,h)anthracene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Diethy1 phthalate NA NA NA NA 170 <10 <10 <10 <10.8 <10 <10 !
Dimethyl phthalate NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Di-n-butyl phthalate NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Di-n-octvl phthalate NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Fluoranthene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Fluorene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Hexachlorobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Hexachlorobutadiene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Hexachlorocvclopentadiene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Hexachloroethane NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Indeno(1.2.3-cd)pyrene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Isophorone NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Naphthalene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Nitrobenzene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
N-Nitrosodimethylamine NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
N-Nitrosodi-n-propylamine NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
N-Nitrosodiphenylamine NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Pentachlorophenol NA NA NA NA <250 <10 <10 <10 <10.8 <10 <10
Phenanthrene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Phenol NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Pyrene NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
Pvridine NA NA NA NA <50 <10 <10 <10 <10.8 <10 <10
1 Historic values reported for Gross Alpha from 1987 and 2003 are total gross alpha reported in pCi/L. All other gross alpha data are reported as Gross Alpha minus Rn &
U.
Ch ~
Major Ions (mWJ) 2007
Carbonate ND
Bicarbonate ND
Calcium 572
Chloride 3700
Fluoride 3.3
Magnesium 4100
Nitrogen-Ammonia 4020
Nitrogen-Nitrate 30.9
Potassium 636
Sodium 4050
Sulfate 60600
gH (s.u.) 3.18
TDS 84300
Conductivity_(umhos/cm) NA
Metals (ug/1)
Arsenic 26900
Beryllium 298
Cadmium 5500
Chromium 2750
Cobalt 46500
Copper 106000
Iron 2770000
Lead 566
Manganese 117000
Mercury ND
Molybdenum 4080
Nickel 123000
Selenium 422
Silver ND
Thallium 361
Tin ND
Uranium 23000
Vanadium 409000
Zinc 767000
Radiologies (pCi/1)
Gross Alpha 1290
VOCS (ug{L)
Acetone 550
Benzene ND
Carbon tetrachloride ND
Chloroform 20
Chloromethane 1.8
MEK 65
------·---
Cell 2 Slimes Drain
I and Radiolo2ical Ch
2008 2009 2010
ND <1 <1
ND <1 <1
528 508 496
3860 2750 3510
ND <0.1 2.4
4030 3750 3790
3620 3240 3820
20.3 38 126
560 689 620
4600 4410 4770
74000 72200 63700
3.24 3.11 3.39
74600 84100 79900
NA 88700 60200
19300 14200 23500
245 271 267
5840 5510 6370
2450 2230 2510
43800 38700 48200
154000 170000 148000
terisf
2011
<1
<1
474
3110
2.1
3640
2940
38
636
4590
64200
3.18
80200
51400
17800
231
5580
2380
42500
132000
3310000 3230000 2720000 2960000
528 403 586 501
130000 160000 144000 123000
ND <0.5 <4 11.1
3190 2240 4630 3510
122000 108000 126000 111000
647 726 844 714
ND <10 <10 <10
703 368 470 371
ND <100 <100 <100
29200 29900 30600 27100
463000 536000 469000 454000
750000 582000 652000 574000
1570 1580 1000 1230
410 570 460 690
ND <1 <1 <1
ND <1 <1 <1
17 16 15 20
ND 2.2 2.3 2
ND 100 83 130
2012 2013 2014
<1 <1 <1
<1 <1 <1
462 465 322
3730 3270 3720
1.32 _j61 130
3760 3320 2780
3540 1880 3500
27 47.2 35.0
611 622 489
4380 3980 3130
58300 83700 62200
3.0 3.02 3.1
83800 92200 87000
52900 51100 54100
19400 21000 19800
251 262 197
5290 5780 6480
2350 2290 1630
48700 44900 46700
138000 137000 126000
2850000 2810000 2180000
619 515 638
141000 122000 98000
1.9 <0.5 <0.0020
3610 3650 4250
125000 108000 127000
711 678 1020
<10 <10 <100
338 278 402
<100 <100 <17000
33400 22800 26400
475000 452000 497000
639000 631000 405000
1370 2270 6890 (2400)*
600 384 <700
<1 <1 <5.0
<1 <1 <5.0
16 21.4 <70.0
3 2.04 <30.0
100 95.5 <4000
Cell 2 Slimes Drain
R ------------------------~ -------------------
Major Ions (mWJ) 2007 2008 2009 2010 2011 2012 2013 2014
Methylene Chloride ND ND <1 <1 <1 <1 <1 <5.0
Na,phthalene 14 7.5 16 17 13 12 16.8 <100
Tetrahvdrofuran 15 NA <100 <10 <10 3.2 3.98 <46.0
Toluene 1.7 ND 2.6 2.6 3 2 3.23 <1000
Xylenes 1.5 ND <1 2.2 <1 2 5.97 <10000
SVOCS (ug/L)
1 ,2,4-Trich1orobenzene NA NA <11 <10 <10 <10 <10 <10
1.2-Dichlorobenzene NA NA <11 <10 <10 <10 <10 <10
1 ,3-Dich1orobenzene NA NA <11 <10 <10 <10 <10 <10
1 A-Dichlorobenzene NA NA <11 <10 <10 <10 <10 <10
1-Methylnaphthalene NA NA <11 <10 <10 <10 <10 11
2,4,5-Trichlorophenol NA NA <11 <10 <10 <10 <10 <10 I
2,4.6-Trichlorophenol NA NA <11 <10 <10 <10 <10 <10
2,4-Dichlorophenol NA NA <11 <10 <10 <10 <10 <10
2,4-Dimethvlphenol NA NA <51 <20 <20 <10 <10 <10 I
2.4-Dinitrophenol NA NA <11 <10 <10 <20 <20 <20
2,4-Dini trotoluene NA NA <11 <10 <10 <10 <10 <10
2,6-Dinitrotoluene NA NA <11 <10 <10 <10 <10 <10 '
2-Chloronaphthalene NA NA <11 <10 <10 <10 <10 <10
2-Chlorophenol NA NA <11 <10 <10 <10 <10 <10
2-Methylnaphthalene NA NA <11 <10 <10 <10 <10 11
2-Methylphenol NA NA <11 <10 <10 <10 <10 <10
2-Nitrophenol NA NA <11 <10 <10 <10 <10 <10
3&4-Methvlpheno1 NA NA <21 <10 <10 <10 <10 <10
3,3 '-Dichlorobenzidine NA NA <51 <10 <10 <10 <10 <10
4.6-Dinitro-2-methvlpheno1 NA NA <11 <10 <10 <10 <10 <10
4-Bromophenyl phenyl ether NA NA <11 <10 <10 <10 <10 <10
4-Chloro-3-methvlphenol NA NA <11 <10 <10 <10 <10 <10 I
4-Chlorophenyl phenyl ether NA NA <51 <10 <10 <10 <10 <10
4-Ni trQIJhenol NA NA <11 <10 <10 <10 <10 <10 I
Acenaphthene NA NA <11 <10 <10 <10 <10 <10
Acenaphthvlene NA NA <11 <10 <10 <10 <10 <10
Anthracene NA NA <11 <10 <10 <10 <10 <10
Azobenzene NA NA <11 <10 <10 <10 <10 <10
Benz(a)anthracene NA NA <21 <10 <10 <10 <10 <10
Benzidine NA NA <11 <10 <10 <10 <10 <10
Benzo( a)pyrene NA NA <11 <10 <10 <10 <10 <10
Benzo(b)fluoranthene NA NA <11 <10 <10 <10 <10 <10
Benzo(g,h.i)pervlene NA NA <11 <10 <10 <10 <10 <10
Benzo(k)fluoranthene NA NA <11 <10 <10 <10 <10 <10
Bis(2-chloroethoxy)methane NA NA <11 <10 <10 <10 <10 <10
Bis(2-chloroethvl) ether NA NA <11 <10 <10 <10 <10 <10
Bis(2-chloroisopropyl) ether NA NA <11 <10 <10 <10 <10 <10
Bis(2-ethvlhexyl) phthalate NA NA <11 <10 <10 <10 <10 <10
Butyl benzyl phthalate NA NA <11 <10 <10 <10 <10 <10
Major Ions (mWJ.)
Chrysene
Dibenz(a,h)anthracene
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno( l .2.3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Ch -----
2007
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
~---
Cell2 Slimes Drain
d Radioi<M!ital Ch
2008 2009 2010
NA <11 <10
NA <11 <10
NA <11 <10
NA <11 <10
NA <11 <10
NA <11 <10
NA <11 <10
NA <11 <10
NA <11 <10
NA <11 <10
NA <11 <10
NA <11 <10
NA <II <10
NA <11 <10
NA <11 <10
NA <11 <10
NA <11 <10
NA <11 <10
NA <51 <10
NA <11 <10
NA <11 <10
NA <11 10.7
NA <11 <10
NA <11 <10
* Sample was reanalyzed due to comparability with the duplicate sample. The reanalysis data are in (parenthesis).
2011 2012 2013 2014
<10 <10 <10 <10
<10 <10 <10 <10
<10 <10 <10 <10
<10 <10 <10 <10
<10 <10 <10 <10
<10 <10 <10 <10
<10 <10 <10 <10
<10 <10 <10 <10
<10 <10 <10 <10
<10 <10 <10 <10
<10 <10 <10 <10 I
<10 <10 <10 <10 I
<10 <10 <10 <10
<10 <10 <10 <10
<10 <10 <10 <10
<10 <10 <10 <10 I
<10 <10 <10 <10 i
<10 <10 <10 <10 I
<10 <10 <10 <10 I
<10 <10 <10 <10
<10 <10 <10 <10 I
<10 <10 <10 <10
<10 <10 <10 <10 I
<10 <10 <10 <10
Cell2 LDS
Ch ---------I and RadiolomcaJ Ch terisf
Constituent 2009 2010 2011 2012 2013 2014 I
Major Ions (mg/1) -Carbonate <1 <1
'
Bicarbonate 168 324
Calcium 711 615
Chloride 1750 1360
Fluoride 0.4 0.4
Ma~nesium 596 454
Nitrogen-Ammonia 32.6 0.7 Not Sampled Not Sampled Not Sampled Not Sampled Nitrogen-Nitrate 2.8 2.2
Potassium 22 13.0
Sodium 412 318
Sulfate 2700 1780
pH (s.u.) 6.60 7.36
TDS 6750 5310
Conductivity (umhos/cm) 11000 6500
Metals (ug/1)
Arsenic <5 <5
I Beryllium <0.50 <0.50
Cadmium 33.4 1.10
Chromium <25 <25
' Cobalt 314 <10
Copper 59 12
Iron 208 37
Lead <1.0 <1.0
Manganese 1810 395
Mercury <0.50 0.52 Not Sampled Not Sampled Not Sampled Not Sampled
Molybdenum 21 13
Nickel 948 <20
Selenium 7.9 9.4
Silver <10 <10
Thallium 0.92 <0.50
Tin <100 <100
Uranium 83.8 79.6
Vanadium 22 <15
Zinc 4220 78
Radiolos:ics {pCi/1)
Gross Alpha 13.5 7.3 Not Sampled Not Sampled Not Sampled Not Sampled
VOCS (ug/L)
Acetone <20 <20
Benzene <1 <1
Carbon tetrachloride <1 <1 Not Sampled Not Sampled Not Sampled Not Sampled
Chloroform <1 <1
Chloromethane <1 <1
Cell2 LDS
Ch I and Radiolo!!icaJ Ch terisf ~--~-~-----~-~-
Constituent 2009 2010 2011 2012 2013 2014
Major Ions (JD211)
MEK <20 <20
Methylene Chloride <1 <1
Naphthalene <1 <1
Tetrahydrofuran <100 6.13
Toluene <1 <1
Xylenes <1 <1
SVOCS (ug!L)
1 ,2,4-Trichlorobenzene NA <10
1.2-Dichlorobenzene NA <10
1 ,3-Dichlorobenzene NA <10
1.4-Dichlorobenzene NA <10
1-Methylnaphthalene NA <10
2,4,5-Trichlorophenol NA <10
2,4,6-Trichlorophenol NA <10
2,4-Dichlorophenol NA <10
2,4-Dimethylphenol NA <10
2,4-Dinitrophenol NA <20
2,4-Dinitrotoluene NA <10
2.6-Dinitrotoluene NA <10
2-Chloronaphthalene NA <10
2-Chlorophenol NA <1 0
2-Methylnaphthalene NA <10
2-Methvlphenol NA <10
2-Nitrophenol NA <10
3&4-Methylphenol NA <10
3,3 '-Dichlorobenzidine NA <10 Not Sampled Not Sampled Not Sampled Not Sampled
4.6-Dinitro-2-methylphenol NA <10
4-Bromo_phenylphenyl ether NA <10
4-Chloro-3-methvlphenol NA <10
4-Chlorophenyl phenyl ether NA <10
4-Nitrophenol NA <10
Acenaphthene NA <10
Acenaphthylene NA <10
Anthracene NA <10
Azobenzene NA <10
Benz(a)anthracene NA <10
Benzidine NA <10
Benzo(a)pyrene NA <10
Benzo(b )fluoranthene NA <10
Benzo(g,h,i)perylene NA <10
Benzo(k)lluornnthene NA <10
Bis(2-chloroethoxy)methane NA <10
Bis(2-chloroethyl) ether NA <10
Bis(2-chloroisopropyl) ether NA <10 -
Constituent
Major Ions (mJ11)
Bis(2-ethylhexyl) phthalate
Butyl benzyl phthalate
Chrvsene
Dibenz(a.h)anthracene
Diethvl phthalate
Dimethyl ohthalate
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocvclopentadiene
Hexachloroethane
lndeno(l ,2,3-cd)pyrene
lsophorone
Naphthalene
Nitrobenzene
N-Nitrosodimethvlamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenvlamine
Pentachlorophenol
Phenanthrene
Phenol
Pvrene
Pyridine
--
Cell2 LDS
Chemical and Radiolotrical Ch
2009 2010
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
NA <10
2011 2012 -2013 2014
Cell3
Ch I and Radiololrlcal Ch terist'
Constituent 1987 2003 2007 2008 2009 2010 2011 2012 2013 2013 2014 (Avg) (Avg) (resample)
Major Ions (mWI)
Carbonate NA <I ND ND <1 <1 <I <1 <I NS <I
Bicarbonate <5 NA ND ND <1 <1 <I <1 <1 NS <1
Calcium 300 418 887 478 628 560 200 591 586 NS 294
Chloride NA 2460 15965 15400 17200 3470 40400 8880 38400 NS 7200
Fluoride <100 667 42.8 1.4 0.6 54.8 64.1 2300 12400 NS 1330
Magnesium 5400 3386 15767 13100 17100 2500 22100 5680 15400 NS 1910
Nitrogen-Ammonia 13900 1302 13867 9010 21600 2650 6470 6840 100 NS 3030
Nitrogen-Nitrate <100 20 102 44 142 26 261 64 277 NS 59.5
Potassium NA 254 6657 4760 3820 782 2590 1190 2110 NS 386
Sodium 5900 3198 25583 22900 28600 5620 47900 6660 34400 NS 3630
Sulfate 180000 33400 173667 167000 214000 40400 197000 80000 440000 NS 37000
pH (s.u.) 0.82 2.28 1.60 1.79 1.4 2.18 1.27 2.4 1.05 NS 2.2
TDS 189000 51633 228500 193000 243000 56200 296000 120000 410000 NS 70100
Conductivity (umhos/cm) NA NA NA NA 304000 59800 86400 80300 84300 NS 56200
MetalS (ug/1)
Arsenic 163000 32867 256500 489000 ND 52900 263000 4340 66000 NS 2920
Beryllium 540 430 913 840 905 206 1570 678 2570 NS 222
Cadmium 2600 1958 9260 15400 ND 1960 12200 3460 24000 NS 2550
Chromium 12000 3742 14883 12800 ND 3360 22800 10900 30600 NS 2380
Cobalt 48000 NA 82783 57000 ND 13000 76000 76100 99700 NS 20800
Copper 360000 87333 505000 345000 ND 89000 768000 379000 954000 NS 139000
Iron 2100000 1278333 4874500 4400000 5970000 1460000 1.02E+7 3400000 9700000 NS 688000
Lead <20000 2507 9647 16900 ND 17200 16700 1860 14400 NS 1900
Manganese 82000 144000 496833 313000 ND 101000 587000 3110000 2470000 NS 214000
Mercury ND NA ND 16 ND <4 30.9 9.6 21.6 NS 2.4
Molybdenum 52000 12250 122167 209000 14 21300 96200 790 56100 NS 2930
Nickel 170000 20917 131833 241000 ND 23800 75800 150000 122000 NS 44900
Selenium <2000 910 5856 10200 NO 3080 6900 2460 7060 NS 1370
Silver <2500 NA 305 1010 ND 101 792 1850 3380 NS 329
Thallium 4700 NA 446 1200 ND 190 518 1080 694 NS 290
Tin NA NA 1090 1070 NO 155 325 <100 <100 NS <17000
Uranium 118000 67833 332333 636000 3690 180000 458000 835000 1200000 NS 134000
Vanadium 210000 158333 935000 1130000 ND 692000 2370000 836000 3220000 NS 454000
Zinc 590000 NA 748833 515000 ND 134000 726000 652000 1430000 NS 155000
Radiololtics (pCi/1)
Gross Alpha NA 1015831 16533 21700 17000 4030 11100 1530 81900 NS 19700
VOCS(uJVL) I
Acetone 28 NA 80 100 67 37 330 64 302 159 <700
Benzene <5 NA ND NO <1 <1 <1 <1 <5 <1 <5.0
Carbon tetrachloride <5 NA ND NO <1 <1 <1 <1 <5 <1 <5.0
Chloroform 6 NA ND 11 4.2 2.6 31 2 56.3 21 <70.0
Chloromethane NA NA ND ND 1.4 1.8 3.5 1 <5 2.58 <30.0
MEK NA NA ND ND <1 <1 67 <20 <100 24.5 <4000
Cell3
Ch I and Radio1o2ica1 Ch terisf
Constituent 1987 2003 2007 2008 2009 2010 2011 2012 2013 2013 2014 (Avg) (Avg) (resample)
Major Ions (mWJ)
Methylene Chloride 10 NA ND ND <I <I 7.4 <1 6.95 <I <5.0
Naphthalene <10000 NA ND <10 <I 2.1 1.2 <I <5 <1 <100
Tetrahydrofuran NA NA 150 <20 <100 <10 <10 <1 <5 <I <46.0
Toluene <5 NA ND ND <1 <1 <1 <I <5 <I <1000
Xylenes <5 NA ND ND <1 <1 <I <I <5 <I <10000
SVOCS (oWl.)
1.2.4-Trichlorobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
I ,2-Dichlorobenzene NA NA NA NA <II <10 <10 <10 <10.5 <10 <10
1.3-Dichlorobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
1,4-Dichlorobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
1-Methylnaphthalene NA NA NA NA <11 <10 <10 <LO <10.5 <10 <10
2,4,5-Trichlorophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
2.4.6-Trichlorophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
2.4-Dichlorophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
2,4-Dimethylphenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
2.4-Dinitrophenol NA NA NA NA <53 <20 <20 <20 <21.1 <20 <20
2,4-Dinitrotoluene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
2,6-Dinitrotoluene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
2-Chloronaphthalene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
2-Chlorophenol NA NA NA NA <II <10 <10 <10 <10.5 <10 <10
2-Methvlnaphthalene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
2-Methvlphenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
2-Nitrophenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
3&4-Methy1pheno1 NA NA NA NA <1 1 <10 <10 <LO <10.5 <10 <10
3,3 '-Dichlorobenzidine NA NA NA NA <21 <10 <10 <10 <10.5 <10 <10
4,6-Dinitro-2-methy1pheno1 NA NA NA NA <53 <10 <10 <10 <10.5 <10 <10
4-Bromophenyl phenyl ether NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
4-Chloro-3-methvlphenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
4-Chlorophenyl phenyl ether NA NA NA NA <11 I <10 <10 <10 <10.5 <10 <10
4-Nitrophenol NA NA NA NA <53 <10 <10 <LO <10.5 <10 <10
Acenaphthene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Acenaphthylene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Anthracene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Azobenzene NA NA NA NA <1 1 <10 <10 <10 <10.5 <10 <10
Benz(~)anthracene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Benzidine NA NA NA NA <21 <10 <10 <10 <10.5 <10 <10
Benzo(a)pyrene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Benzo(b )fluoranthene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Benzo(g,h,i)pervlene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Benzo(k)fluoranthene NA NA NA NA <1 1 <10 <10 <10 <10.5 <10 <10
Bis(2-chloroethoxy)methane NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Bis(2-chloroethyl) ether NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Bis(2-chloroisopropyl) ether NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Cell3
Ch I and Radiolo!!ical Ch terisf ·-
Constituent 1987 2003 2007 2008 2009 2010 2011 2012 2013 2013 2014 (Avg) (Avg) (resample)
Major Ions (mgll)
Bis(2-ethvlhexvl) phthalate NA NA NA NA <11 10.6 <10 <10 <10.5 <10 <10
Butyl benzyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Chrysene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Dibenz(a,h)anthracene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Diethyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Dimethyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Di-n-butyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Di-n-octyl phthalate NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Fluoranthene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Fluorene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Hexachlorobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Hexachlorobutadiene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Hexachlorocyclopentadiene NA NA NA NA <11 <10 <LO <10 <10.5 <10 <10
Hexachloroethane NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
lndeno(l ,2,3-cd)pyrene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Isophorone NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Naphthalene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Nitrobenzene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
N-Nitrosodimethylamine NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
N-Nitrosodi-n::JJ.r~vlamine NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
N-Nitrosodiphenylamine NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Pentachlorophenol NA NA NA NA <53 <10 <10 <10 <10.5 <10 <10
Phenanthrene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Phenol NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Pxrene NA NA NA NA <11 <10 <10 <10 <10.5 <10 <10
Pyridine NA NA NA NA .. <11 <10 <10 <10 <10.5 <10 <10
1 Historic values reported for Gross Alpha from 1987 and 2003 are total gross alpha reported in pCi!L. All other gross alpha data are reported as Gross Alpha minus Rn &
u.
Cell4A
Ch I and Racliolol!ical Ch terisf
Constituent 2009 2010 2011 2012 2013 2014
Ma.ior Ions (mg/ll I
Carbonate <1 <1 <1 <I <1 <I
Bicarbonate <1 <I <1 <I <1 <I
Calcium 627 598 558 591 668 445
Chloride 4650 7350 5870 4980 4530 5900
Fluoride 0.3 21.6 30.6 43 1130 1290
Magnesium 3250 4940 4720 2230 3660 2990
Nitrogen-Ammonia 3140 5230 4930 1540 1340 2730
Nitrogen-Nitrate 28 52 44 27 38.2 39.5
Potassium 980 1440 1450 558 773 724
Sodium 5980 11300 11400 7130 6860 7190
Sulfate 67600 87100 267000 64900 83300 64900
pH (s.u.) 1.40 1.99 1.73 1.2 1.47 1.7
TDS 81400 107000 108000 76000 90000 97000
Conductivity (umbos/em) 131000 101000 82100 78100 66300 73000
Metals (ug/1)
Arsenic 626000 109000 86600 60500 73700 70000
Beryllium 296 215 323 167 247 190
Cadmium 1920 3670 2190 844 1450 1780
Chromium 3220 7500 5900 5990 5220 4620
Cobalt 9440 26500 22500 22900 22900 27500
Copper 99200 168000 181000 433000 540000 556000
Iron 2360000 2920000 3390000 3190000 2620000 2280000
Lead 5360 11800 11000 5270 11500 14800
Manganese 178000 209000 131000 112000 143000 120000
Mercury 1.19 <4 15.2 2.4 0.786 2.5
Molybdenum 24300 43800 24200 58200 25500 40600
Nickel 17100 40900 43500 41300 43300 54100
Selenium 4620 5810 4460 1310 2080 2000
Silver 78 193 216 127 144 197
Thallium 162 350 410 250 256 376
Tin 257 378 319 169 118 <17000
Uranium 118000 217000 153000 91000 112000 159000
Vanadium 918000 1090000 730000 237000 461000 535000
Zinc 142000 224000 286000 200000 183000 169000
Radiolo!tics {pCi/l)
Gross Alpha 8910 3400 8290 16300 15800 240000
VOCS (ug!L)
Acetone 60 55 100 25 28.4 <700
Benzene <1 <1 <1 <1 <1 <5.0
Carbon tetrachloride <I <1 <1 <1 <I <5.0
Chloroform 4.0 8.5 10 <1 <1 <70.0
Chloromethane 3.4 5.5 7.9 <I <1 <30.0
MEK <I <1 <1 <I <20 <4000
Methvlene Chloride <I <1 <1 <20 <1 <5.0
Ceii4A
----------~--------------- ------------ ----- -Ch I and Radiolo2:ical Ch terisf
Constituent 2009 2010 2011 2012 2013 2014
Major Ions (OWl)
Naphthalene 1.8 <1 <1 <I <1 <100
Tetrahydrofuran <100 <10 <10 1.36 <1 <46.0
Toluene <I <1 <I <1 <I <1000
Xylenes <I <1 <1 <I <1 <10000
svocs (oWl)
1.2.4-Trichlorobenzene <11 <10 <10 <10 <10 <10
1 ,2-Dichlorobenzene <11 <10 <10 <10 <10 <10
1,3-Dichlorobenzene <11 <10 <10 <10 <10 <10
1.4-Dichlorobenzene <II <10 <10 <10 <10 <10
1-Methylnaphthalene <11 <10 <10 <10 <10 <10
2.4.5-Trichlorophenol <11 <10 <10 <10 <10 <10
2,4,6-Trichlorophenol <11 <10 <10 <10 <10 <10
2.4-Dichlorophenol <11 <10 <10 <10 <10 <10
2,4-Dimethylphenol <11 <10 <10 <10 <10 <10
2.4-Dinitrophenol <53 <20 <20 <20 <20 <20
2,4-Dinitrotoluene <11 <10 <10 <10 <10 <10
2,6-Dinitrotoluene <11 <10 <10 <10 <10 <10
2-Chloronaphthalene <11 <10 <10 <10 <10 <10
2-Chlorophenol <11 <10 <10 <10 <10 <10
2-Methy1naphtha1ene <11 <10 <10 <10 <10 <10
2-Methy!pheno1 <11 <10 <10 <10 <10 <10
2-Nitrophenol <11 <10 <10 <10 <10 <10
3&4-Methylphenol <11 <10 <10 <10 <10 <10
3.3 '-Dichlorobenzidine <21 <10 <10 <10 <10 <10
4,6-Dinitro-2-methylphenol <53 <10 <10 <10 <10 <10
4-Bromophenyl phenyl ether <II <10 <10 <10 <10 <10
4-Chloro-3-methylphenol <11 <10 <10 <10 <10 <10
4-Ch1orophenyl phenyl ether <11 <10 <10 <10 <10 <10
4-Nitrophenol <53 <10 <10 <10 <10 <10
Acenaphthene <11 <10 <10 <10 <10 <10
Acenaphthylene <11 <10 <10 <10 <10 <10
Anthracene <11 <10 <10 <10 <10 <10
Azobenzene <11 <10 <10 <10 <10 <10
Benz( a )anthracene <11 <10 <10 <10 <10 <10
Benzidine <21 <10 <10 <10 <10 <10
Benzo(a)pyrene <11 <10 <10 <10 <10 <10
Benzo(b )fluoranthene <11 <10 <10 <10 <10 <10
Benzo(g,h,i)perylene <11 <10 <10 <10 <10 <10
Benzo(k)fluoranthene <11 <10 <10 <10 <10 <10
Bis(2-chloroethoxy)methane <11 <10 <10 <10 <10 <10
Bis(2-chloroethyl) ether <11 <10 <10 <10 <10 <10
Bis(2-chloroisopropyl) ether <11 <10 <10 <10 <10 <10
Bis(2-ethylhexyl) phthalate <11 19.6 <10 <10 <10 <10
Butyl benzyl phthalate <11 <10 <10 <10 <10 <10
Chrysene <11 <10 <10 <10 <10 <10
Cell4A
Ch I and Radioloe:ical Ch terisf
Constituent 2009 2010 -2011 2012 2013 2014
Major Ions (01211)
Dibenz(a.h)anthracene <11 <10 <10 <10 <10 <10
Diethyl phthalate <11 <10 <10 <10 <10 <10
Dimethyl phthalate <11 <10 <10 <10 <10 <10
Di-n-butyl phthalate <11 <10 <10 <10 <10 <10
Di-n-octyl phthalate <II <10 <10 <10 <10 <10
Fluoranthene <II <10 <10 <10 <10 <10
Fluorene <11 <10 <10 <10 <10 <10
Hexachlorobenzene <11 <10 <10 <10 <10 <10
Hexachlorobutadiene <11 <10 <10 <10 <10 <10
Hexachlorocyclopentadiene <11 <10 <10 <10 <10 <10
Hexachloroethane <II <10 <10 <10 <10 <10
Indeno( 1.2.3-cd)pyrene <11 <10 <10 <10 <10 <10
lsophorone <11 <10 <10 <10 <10 <10
Naphthalene <11 <10 <10 <10 <10 <10
Nitrobenzene <11 <10 <10 <10 <10 <10
N-Nitrosodirnethvlarnine <11 <10 <10 <10 <10 <10
N-Nitrosodi-n~prQQYlarnine <II <10 <10 <10 <10 <10
N-Nitrosodiphenylarnine <11 <10 <10 <10 <10 <10
Pentachlorophenol <53 <10 <10 <10 <10 <10
Phenanthrene <11 <10 <10 <10 <10 <10
Phenol <11 <10 <10 <10 <10 <10
Pyrene <II <10 <10 <10 <10 <10
Pyridine <11 <10 <10 <10 <10 <10
Cell4A LDS
Chemical and Radiological Characteristics
Constituent 2009 2010 I 2011 2012 2013 2014
Major Ions (mWI)
Carbonate <1 <1 <1 <1 <1 <1
Bicarbonate <1 <1 <1 <1 <1 <1
Calcium 558 474 470 453 429 336
Chloride 7570 4670 6040 2710 I 1910 4200
Fluoride 0.7 39.4 46 27 1970 1320
Magnesium 6390 3240 5100 2070 1710 2690
Nitrogen-Ammonia 4480 2290 3480 1320 1010 2920
Nitrogen-Nitrate 69 183 94 15 28.9 39.0
Potassium 1960 934 1500 503 305 415
Sodium 12600 6700 11000 3500 2930 4190
Sulfate 92400 41700 77400 39600 31400 56000
pH (s.u.) 1.98 2.53 2.32 2.1 2.32 2.4
TDS 117000 56900 93800 55400 49700 81900
Conductivity (umbos/em) 150000 49000 66600 39600 31300 53600
Metals (uj!/1)
Arsenic I 33000 54000 74700 44100 35700 51200
Beryllium 536 295 367 180 188 185
Cadmium 4010 2650 3160 921 1170 4720
Chromium 9140 3890 5940 3930 2630 2780
Cobalt 37300 15200 21700 22300 44300 41200
Copper 222000 116000 150000 481000 754000 439000
Iron 3940000 1420000 2530000 2460000 1370000 1850000
Lead 5270 3400 4520 2300 165 991
Manganese 389000 157000 207000 95200 86300 98600
Mereu!}' 2.66 6.2 14.7 0.7 <0.5 <0.0020
Molybdenum 49200 23900 29300 10200 1200 3970
Nickel 43900 23900 29600 35000 54600 99300
Selenium 5250 2820 3780 1260 1020 2170
Silver 204 62 127 44 24.8 <100
Thallium 252 194 290 332 171 522
Tin 504 180 119 <100 <100 <17000
Uranium 284000 145000 168000 90200 75000 82200
Vanadium 1150000 518000 770000 240000 157000 510000
Zinc 298000 152000 204000 181000 163000 306000
Radiolo~ics (pCi/l)
Gross Alpha 7020 3230 7440 4730 6930 61800
VOCS (ue/1.) I
Acetone 240 130 120 55 57 <700 I
Benzene <I <I <1 <1 <1 <5.0 j
Carbon tetrachloride <1 <I <1 <I <I <5.0 J
Cell4A LDS
--------------------~--------------------------Ch I and Radiolol!ical Ch terisf
Constituent 2009 2010 2011 2012 2013 2014
Ma.ior Ions (nu11) I
Chloroform 23 52 26 42 110 95.0
Chloromethane 7.9 13 3.8 6 9.93 <30.0
MEK 78 50 82 36 <20 <4000
Methylene Chloride <1 <I <1 <1 <1 <5.0
Naphthalene <1 1.5 <1 I 2.35 <100
Tetrahydrofuran 140 158 102 117 39.1 <46.0
Toluene <1 <1 <1 <1 <1 <1000
Xy1enes <1 <1 <1 <1 <1 <10000
SVOCS (ug!L)
1 ,2,4-Trichlorobenzene <11 <10 <10 <10 <10 <10
1.2-Dichlorobenzene <11 <10 <10 <10 <10 <10
1,3-Dichlorobenzene <11 <10 <10 <10 <10 <10
1.4-Dich1orobenzene <11 <10 <10 <10 <10 <10
1-Methylnaphtha1ene <11 <10 <10 <10 <10 <10
2,4,5-Trich1oropheno1 <11 <10 <10 <10 <10 <10
2.4.6-Trichloro_pheno1 <11 <10 <10 <10 <10 <10
2.4-Dich1oropheno1 <11 <10 <10 <10 <10 <10
2.4-Dimethy\phenol <11 <10 <10 <10 <10 <10
2,4-Dinitropheno1 <54 <20 <20 <20 <20 <20
2.4-Dinitrotoluene <ll <10 <10 <10 <10 <10
2,6-Dinitrotoluene <11 <10 <10 <10 <10 <10
2-Ch1oronaphthalene <11 <10 <10 <10 <10 <10
2-Chloropheno1 <II <10 <10 <10 <10 <10
2-Methylnaphthalene <11 <10 <10 <10 <10 <10
2-Methvlphenol <11 <10 <10 <10 <10 <10
2-Nitrophenol <11 <10 <10 <10 <10 <10
3&4-Methylphenol <11 <10 <10 <10 <10 <10
3.3 '-Dichlorobenzidine <22 <10 <10 <10 <10 <10
' 4 .. 6-Dinitro-2-methvliJhenol <54 <10 <10 <10 <10 <10
4-Bromophenyl phenyl ether <11 <10 <10 <10 <10 <10
4-Chloro-3-methvlphenol <11 <10 <10 <10 <10 <10
4-Ch1orophenyl phenyl ether <11 <10 <10 <10 <10 <10
4-Nitrophenol <54 <10 <10 <10 <10 <10
Acenaphthene <11 <10 <10 <10 <10 <10
Acenaphthv1ene <11 <10 <10 <10 <10 <10
Anthracene <11 <10 <10 <10 <10 <10
Azobenzene <11 <10 <10 <10 <10 <10
Benz(a)anthracene <11 <10 <10 <10 <10 <10
Benzidine <22 <10 <10 <10 <10 <10
Benzo(a)pyrene <11 <10 <10 <10 <10 <10
Benzo(b )fluoranthene <11 <10 <10 <10 <10 <10
Benzo( g_.h.i)pervlene <11 <10 <10 <10 <10 <10
Benzo(k)fluoranthene <11 <10 <10 <10 <10 <10
Bis(2-ch1oroethoxy)methane <11 <10 <10 <10 <10 <10
Bis(2-chloroethyl) ether <11 <10 <10 <10 <10 <10
Cell4ALDS
Ch ---~ ------------d Radioloeical Ch ----terisf ---.
Constituent 2009 2010 2011 2012 2013 2014
Ma.ior Ions (J.I121l)
Bis(2-chloroisopropyl) ether <11 <10 <10 <10 <10 <10
Bis(2-ethylhexyl) phthalate <11 54.9 54.9 16.6 <10 <10
Butvl benzyLphthalate <11 <10 <10 <10 <10 <10
Chrysene <11 <10 <10 <10 <10 <10
Dibenz(a,h)anthracene <11 <10 <10 <10 <10 <10 I
Diethvl phthalate <11 <10 <10 <10 I <10 <10
Dimethyl phthalate <11 <10 <10 <10 <10 <10
Di-n-butvl_phthalate <11 <10 <10 <10 <10 <10
Di-n-octvl phthalate <11 <10 <10 <10 <10 <10
Fluoranthene <ll <10 <10 <10 <10 <10
Fluorene <11 <10 <10 <10 <10 <10
Hexachlorobenzene <11 <10 <10 <10 <10 <10
Hexachlorobutadiene <ll <10 <10 <10 <10 <10
Hexach1orocyclopentadiene <11 <10 <10 <10 <10 <10
Hexachloroethane <11 <10 <10 <10 <10 <10
lndeno(1 ,2,3-cd)pyrene <11 <10 <10 <10 <10 <10
Isophorone <11 <10 <10 <10 <10 <10
Naphthalene <11 <10 <10 <10 <10 <10
Nitrobenzene <11 <10 <10 <10 <10 <10
N-Nitrosodimethylamine <11 <10 <10 <10 <10 <10
N-Ni trosodi -n-propylami ne <11 <10 <10 <10 <10 <10
N-Nitrosodiphenylamine <11 <10 <10 <10 <10 <10
Pentachlorophenol <54 <10 <10 <10 <10 <10
Phenanthrene <11 <10 <10 <10 <10 <10
Phenol 33 23.5 <10 <10 <10 <10
Pvrene <11 <10 <10 <10 <10 <10
Pyridine <11 <10 <10 --<10 <10 <10
Cell4B
Ch I and R.adioloeical Ch terisf
Constituent 2011 2012 2013 2014
Major Ions (mg/1) -, -
Carbonate <1 <1 <1 <1
Bicarbonate <1 <1 <1 <1
Calcium 570 580 662 366
Chloride 8290 8170 4570 7300
Fluoride 26.7 23.3 1050 1150
Magnesium 3910 4500 3560 3310
Nitrogen-Ammonia 5220 5580 2060 5380
Nitrogen-Nitrate 39 42 51.4 47.0
Potassium 1370 1650 1110 989
Sodium 9050 11700 3150 7100
Sulfate 134000 119000 98100 91500
pH (s.u.) 1.87 1.5 1.65 1.6
TDS 98000 128000 108000 131000
Conductivity (umhos/cm) 76900 86900 72800 90100
Metals (ug/1)
Arsenic 67400 80000 65400 70400
Beryllium 311 356 334 275
Cadmium 1990 2540 1990 2290
Chromium 6860 8280 6390 6940
Cobalt L7800 29300 21300 24600
Copper 193000 340000 340000 368000
Iron 2960000 3580000 2830000 2480000
Lead 9960 11600 9820 10900
Manganese 128000 148000 154000 129000
Mercury 13.7 2.6 1.49 <0.0020
Molybdenum 21400 27600 26100 29000
Nickel 33900 50500 35100 42000
Selenium 4670 4470 3900 5010
Silver 137 169 137 142
Thallium 237 368 243 258
Tin 196 215 163 <17000
Uranium 133000 171000 110000 133000
Vanadium 660000 783000 163000 666000
Zinc 191000 270000 184000 144000
Radiolo~ics (pCi/1)
Gross Alpha 8590 13600 14600 148000
I VOCS (ug/L)
Acetone 130 94 43.5 <700
Benzene <1 <1 <1 <5.0
Carbon tetrachloride <1 <1 <1 <5.0
Chloroform 9.4 4 8.06 <70.0
Chloromethane 8.5 8 7.12 <30.0
MEK <1 <1 <20 <4000
'-
Cell4B
Chemical and Radiolol!ical Ch
Constituent 2011 2012
Major Ions (mWI)
Methylene Chloride <1 <1
Naphthalene <1 <1
Tetrahydrofuran <10 11.1
Toluene <1 <1
Xylenes <1 <I
svocs (U2fl)
1 ,2.4-Trichlorobenzene <10 <10
I ,2-Dichlorobenzene <10 <10
1 ,3-Dichlorobenzene <10 <10
1.4-Dich1orobenzene <10 <10
1-Methylnaphthalene <10 <10
2.4,5-Trichloropheno1 <10 <10
2,4.6-Trichlorophenol <10 <10
2,4-Dichlorophenol <10 <10
2.4-Dimethvlphenol <10 <10
2,4-Dinitrophenol <20 <20
2.4-Dinitrotoluene <10 <10
2,6-Dinitrotoluene <10 <10
2-Chloronaphthalene <10 <10
2-Chloroohenol <10 <10
2-Methylnaphthalene <10 <10
2-Methvlohenol <10 <10
2-Nitrophenol <10 <10
3&4-Methylphenol <10 <10
3.3 '-Dichlorobenzidine <10 <10
4,6-Dinitro-2-methylphenol <10 <10
4-Bromophenvl phenyl ether <10 <10
4-Ch1oro-3-methvlohenol <10 <10
4-Chlorophenyl phenyl ether <10 <10
4-Nitrophenol <10 <10
Acenaphthene <10 <10
Acenaphthylene <10 <10
Anthracene <10 <10
Azobenzene <10 <10
Benz(a)anthracene <10 <10
Benzidine <10 <10
Benzo(a)ovrene <10 <10
Benzo(b )fluoranthene <10 <10
Benzo(g,h,i)perylene <10 <10
Benzo(k)fluoranthene <10 <10
Bis(2-chloroethoxv)methane <10 <10
Bis(2-chloroethyl) ether <10 <10
Bis(2-chloroisopropyl) ether <10 <10
Bis(2-ethylhexvl) phthalate 410 19
Bt1tyl benzyl phthalate <10 <10
2013 2014
'
<1 <5.0
<1 <100
<1 <46.0
<1 <1000
<I <10000
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<20 <20
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 26
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
<10 <10
Ce114B
Chemical and Radiological Characteristics
Constituent 2011 2012 2013 2014
Major Ions (Dl2fl)
Chrvsene <10 <10 <10 <10
Dibenz(a,h)anthracene <10 <10 <10 <10
Diethyl phthalate <LO <10 <10 <10
Dimethyl phthalate <10 <10 <10 <10
Di-n-butyl IJhtha1ate <10 <10 <10 <10
Di-n-octvl phthalate <10 <10 <10 <10
Fluoranthene <10 <10 <10 <10
Fluorene <10 <10 <10 <10
liexachlorobenzene <10 <10 <10 <10
liexachlorobutadiene <10 <10 <10 <10
liexachlorocvclopentadiene <10 <10 <10 <10
liexach1oroethane <10 <10 <10 <10
Indeno(l ,2,3-cd)pyrene <10 <10 <10 <10
Isophorone <10 <10 <10 <10
Nlill_hthalene <10 <10 <10 <10
Nitrobenzene <10 <10 <10 <10
N-Nitrosodimethylamine <10 <10 <10 <10
N-Nitrosodi-n-propy1amine <10 <10 <10 <10
N-Nitrosodiphenvlamine <10 <10 <10 <10
Pentachlorophenol <10 <10 <10 <10
Phenanthrene <10 <10 <10 <10
Phenol <10 <10 <10 <10
Pyrene <10 <10 <10 <10
P_yridine <10 <10 <10 15
Cell4B LDS
------------------------------------------------Ch I and RadioJocicaJ Ch terisf
Constituent 2011 2012 2013 2014
Major Ions (mWl)
Carbonate <1 <1 <1
Bicarbonate <1 <I <1
Calcium 486 456 308
Chloride 3630 6850 6900
Fluoride 28.4 22 970
Magnesium 3230 3360 3400
Nitrogen-Ammonia 4260 4090 Not Sampled -5240
Nitrogen-Nitrate 30 31 dry 43.0
Potassium 1130 1060 952
Sodium 8240 8080 6920
Sulfate 59900 99100 82300
pH (s.u.) 2.23 2.4 2.2
TDS 85800 90200 129000
ConducLivity (umhos/cm). 63000 62400 76300
Metals (uWJ)
Arsenic 54200 41200 67800
Beryllium 274 271 282
Cadmium 1670 1740 2290
Chromium 6250 5930 6160
Cobalt 15600 19000 23300
Copper 176000 181000 308000
Iron 2450000 2120000 2590000
Lead 6060 4420 4120
ManMncse 118000 162000 144000
Mercury 12.3 3 Not Sampled -0.0020
Molybdenum 16700 15000 dry 24300
Nickel 30700 33700 40100
Selenium 3710 2880 4080
Silver 111 117 119
Thallium 179 175 336
Tin 332 <100 <17000
Uranium 111000 132000 143000
Vanadium 518000 428000 671000
Zinc 172000 182000 144000
Radioloeics (pCi/1)
Gross Alpha 6000 7500 Not Sampled-181000 dry
VOCS {ugfL) I
Acetone 390 370 <700
Benzene <1 <I <5.0
Carbon tetrachloride <1 <I Not Sampled -<5.0
Chloroform 20 19 <70.0
Chloromethane II J I dry <30.0
MEK 240 180 <4000
Mer,hylcn~ Chloride <1 <1 <5.0 -----
Celi4B LDS
Chemical and Radiolo~cal Characteristics
Constituent 2011 2012 2013 2014
Ma.i_or Ions (mWi)
Naphthalene <1 <1 <100
Tetrahydrofuran 198 322 75.6
Toluene <1 <1 <1000
Xvlenes <1 <1 <10000 svocs (ug!L)
1.2.4-Trichlorobenzene <10 <10 <10
1 ,2-Dichlorobenzene <10 <10 <10
1 ,3-Dichlorobenzene <10 <10 <10
1.4-Dichlorobenzene <10 <10 <10
1-Methylnaphthalene <10 <10 <10
2.4.5-Trichlorophenol <10 <10 <10
2.4,6-Trichlorophenol <10 <10 <10
2,4-Dichlorophenol <10 <10 <10
2.4-Dimethylphenol <10 <10 <10
2,4-Dinitrophenol <20 <20 <20
2.4-Dini trotoluene <10 <10 <10
2,6-Dinitrotoluene <10 <10 <10
2-Chloronaphthalene <10 <10 <10
2-Chlorophenol <10 <10 <10
2-Methylnaphthalene <10 <10 <10
2-Methvlphenol <10 <10 <10
2-Nitrophenol <10 <10 <10
3&4-Methylphenol <10 <10 <10
3,3'-Dichlorobenzidine <10 <10 Not Sampled-<10
4,6-Dinitro-2-methylphenol <10 <10 <10
4-Bromophenyl phenyl ether <10 <10 dry <10
4-Chloro-3-methylphenol <10 <10 <10
4-ChloroQhenyl phenyl ether <10 <10 <10
4-Nitrophenol <10 <10 <10
Acenaphthene <10 <10 <10
Acenaphthylene <10 <10 <10
Anthracene <10 <10 <10
Azobenzene <10 <10 <10
Benz(a)anthracene <10 <10 <10
Benzidine <10 <10 <10
Benzo(a)pyrene <10 <10 <10
Benzo(b )fluoranthene <10 <10 <10
Benzo(g,h,i)perylene <10 <10 <10
Benzo(k )fl uoranthene <10 <10 <10
Bis(2-chloroethoxy)methane <10 <10 <10
Bis(2-chloroethyl) ether <10 <10 <10
Bis(2-chloroisopropyl) ether <10 <10 <10
Bis(2-ethvlhexvl) phthalate 191 191 27
Butyl benzyl phthalate <10 <10 <10
~--
Chrysene <10 <10 <10
Ce114B LDS
Chemical and Radiol~cal Characteristics
Constituent 2011 r 2012 1 2on 2014
Major Ions (mWi)
Dibenz(a,h)anthracene <10 <10 <10
Diethyl phthalate <10 <10 <10
Dimethyl phthalate <10 <10 <10
Di-n-butyl phthalate <10 <10 <10
Di-n-octyl phthalate <10 <10 <10
Fluoranthene <10 <10 <10
Fluorene <10 <10 <10
Hexachlorobenzene <10 <10 <10
Hexachlorobutadiene <10 <10 <10
Hexachlorocyclopentadiene <10 <10 <10
Hexachloroethane <10 <10 <10
Indeno(_l ,2,3-cd)pyrene <10 <10 <10
lsophorone <10 <10 <10
N~hthalene <10 <10 <10
Nitrobenzene <10 <10 <10
N-Nitrosodimethylarnine <10 <10 <10
N-Nitrosodi-n-propylarnine <10 <10 <10
N-Nitrosodiphenylamine <10 <10 <10
PentachlorQPhenol <10 <10 <10
Phenanthrene <10 <10 <10
Phenol <10 <10 <10
Pyrene <10 <10 <10
Pyridine <10 <10 <10
1980-2003 IUC/NRC Tailin!!S Wast terS l"~*l
~
Constituent Minimum Maximum
pH (Std units) 0.7 2.33
Nutrients (mg!L)
Ammonia (N) 3.0 13900
Nitrite (N) <fOO <100
Nitrate (N) 24 24
Nitrate+Nitrite (Nl 17.0 49.2
Phosphorus -total 88.1 620
TKN (N) 4900 5300
Inor2anics (1112fl )
Bicarbonate (HC03) <5 <5
Bromide <500 <500
Carbonate (C03) <1 <5
Chloride 2110 8000
Cyanide-total 0.022 0.022
Fluoride 0.02 4400
Phosphate <500 <500
Silica 110 400
Sulfate 29800 190000
Sulfide <5 <5
TDS 43100 189000
TOC 76.0 81
TSS 31.0 115
Metals (mWI)
Aluminum 330 2530
Antimony <20 <20
Arsenic 0.3 440
Barium 1.021 0.1
Beryllium 0.347 0.78
Boron 3.5 11.3
Cadmium 1.64 6.6
Calcium 90.0 630
Chromium 1.0 13
Cobalt 14.0 120
Copper 72.2 740
Iron 1080 3400
Gallium <30 <30
Lead 0.21 6.0
Lithium <10 <20
Magnesium 1800 7900
Manganese 74.0 222
Mercury 0.0008 17.6
Molybdenum 0.44 240
Nickel 7.2 370
Potassium 219.0 828
Selenium 0.18 2.4
Silver 0.005 0.14
Sodium 1400 10000
~
---------1980-2003 IUC/NRC Tail' Wast terS *1
Constituent Minimum Maximum
Strontium 3.6 14
Thallium 0.7 45
Tin <5 <5
Titanium 6.5 33.3
Uranium 5.0 154
Vanadium 136 510
Zinc 50 !300
Zirconium 2.3 38.5
Radiolo~ics (pCi/L)
Gross Alpha 14000 189000
Gross Beta 74 116000
Lead-210 680 20700
Thorium-230 3650 76640
Thorium-232 49 121
Polonium-210 1410 1410
Radium-226 40 1690
Radium-228 1.9 I 1.9
Total Radium 42 1700
Sclected VOCs (u2/L) .-
Acetone 28 514
Benzene <5 <5
2-butanone (MEK) 11 15.13
Carbon Disulfide 16 16
Carbon Tetrachloride <5 <5
Chloroform 6 16.84
1. I-Dichloroethane <5 <5
1,2-Dichloroethane <5 <5
Dichloromethane 10 11
Tetrahydofuran N/A N/A
Toluene <5 6.25
VInyl Chloride <10 <10
Xylene (total) <5 <5
Selected Semivolatiles (u2/L)
Benzo(a)py[ene <10 <10
Bis(2-ethylhex.vl)pht.halate 1 1
Chrysene <10 <10
Diethyf phthalate <10 18.1
Dimethy(p_hLhalatc 2.7 2.7
Di-n;butylphthalate 1.08 1.08
Fluoranthene <10 <10
2-Methylnaphthalene <10 <10
Naphthalene 2.44 2.44
Phenol <10 38.4
*Reproduced from the Utah Division of Radiation Control Groundwater Quality Discharge Permit, Statement of Basis for a Uranium Mining Facility at White Mesa, South of Blanding, Utah, dated December I,
2004.
'The data in the Utah Division of Radiation Control Groundwater Quality Discharge Permit, Statement of Basis are based on historical data collected from Cell I, Cell 2, and Cell 3. The date of collection reflects
which cells were operational at the time of sampling. The location of the samples and date of collection is referenced in the Statement of Basis.
TabE
Quality Assurance and Data Validation Tables
Table E-1 Bolding Time Evaluation
Celli Cell2 Cell3 Ceii4A Ceii4A Cell4B Celi4B Cell65
Required Holding Time Tailings Slimes Tailings Tailings LOS Tailings LDS (Duplicate
Fluid Drain Fluid Fluid Fluid lofCe114A\
Carbonate 14 days OK OK OK OK OK OK OK OK
Bicarbonate 14 days OK OK OK OK OK OK OK OK
Calcium 6 months OK OK OK OK OK OK OK OK
Chloride 28 days OK OK OK OK OK OK OK OK
Fluoride 28 days OK OK OK OK OK OK OK OK
Magnesium 6 months OK OK OK OK OK OK OK OK
Nitrogen-Ammonia 28 days OK OK OK OK OK OK OK OK
Nitrogen-Nitrate 28 days OK OK OK OK OK OK OK OK
Potassium 6 months OK OK OK OK OK OK OK OK
Sodium 6 months OK OK OK OK OK OK OK OK
Sulfate 28 days OK OK OK OK OK OK OK OK
pH (pH units) Immediately OK* OK* OK* OK* OK* OK* OK* OK*
TDS 7 days OK OK OK OK OK OK OK OK
Conductivity (umhos/cm) N/A OK OK OK OK OK OK OK OK
6 months (except mercury
Metals which is 28 days) OK OK OK OK OK OK OK OK
Radiologies 6 months OK OK OK OK OK OK OK OK
VOCS (including THF) 14 days OK OK OK OK OK OK OK OK
7 days to extraction/40
svocs days for analysis OK OK OK OK OK OK OK OK
* Per the method, pH should be analyzed within 15 minutes of sample collection. Due to the nature of the tailings matrix, sample
handling in the field is minimized and pH is measured by the laboratory upon receipt. This procedure change was requested by and
approved by DRC.
E-2 Laboratorv Receipt Temperature Check -
WoJ'k. Qrd_er Number/Lab
SeUllli> :R«:!<;eipt T<!:mp
GEL-358469 N/A
CTF-1408830 4.1°C
N/A =These shipments contained samples for the analysis of
gross alpha only. Samples submitted for gross alpha analyses do
not have a sample temperature requirement.
E-3: Analytical Method Check -Routine Samples
Parameter QAP/Permit Method Method Used by Lab
Ammonia (as N) A4500-NH3 G or E350.1 A4500-NH3 G
Nitrate+ Nitrite (as N) E353.1 or E353.2 E353.2
Metals E200.7 or E200.8 E200.7 and E200.8
Gross Alpha E900.0 or E900.1 E900.1
VOCs SW8260B or SW8260C SW8260B
Chloride A4500-Cl B or E300.0 E300.0
Fluoride A4500-F C or E300.0 E300.0
Sulfate A4500-S04 E or E300.0 E300.0
TDS A2540C A2540 C
Carbonate as C03, Bicarbonate as HC03 A2320 B A2320 B
pH A4500 H-B A4500 H-B
Conductivity EPA 120.1 EPA 120.1
SVOCs SW8270D SW8270D
E-4 Reporting Limit Evaluation
Parameter Permit-Specified RL
Ammonia (as N) 25 mg/L
Nitrate+ Nitrite (as N) 10 mg/L
Metals ug/L
Arsenic 50
Beryllium 4
Cadmium 5
Chromium 100
Cobalt 730
Copper 1300
Iron 11000
Lead 15
Manganese 800
Mercury 2
Molybdenum 40
Nickel 100
Selenium 50
Silver 100
Thallium 2
Tin 17000
Uranium 30
Vanadium 60
Zinc 5000
Gross Alpha 15
VOCs ug/L
Acetone 700
Benzene 5
Carbon tetrachloride 5
Chloroform 70
Chloromethane 30
MEK 4000
Methylene Chloride 5
Naphthalene 100
Tetrahydrofuran 46
Toluene 1000
Xylenes 10000
Major Ions
Chloride 1.0 mg/L
Fluoride 4mg/L
Sulfate 1000 mg/L
TDS 1000 mg/L
Carbonate as C03, Bicarbonate as HC03 1*
Calcium, Magnesium, Potassium, Sodium 1*
SVOCs (from the 8270D LLD) ug/L
1 ,2,4-Trichlorobenzene 10
1 ,2-Dichlorobenzene 10
E4R -eportmg L' . E I 1m1t va uation
Parameter Permit-Specified RL
1 ,3-Dichlorobenzene 10
1 ,4-Dichlorobenzene 10
1-Methylnaphthalene 10
2,4,5-Trichlorophenol 10
2,4,6-Trichlorophenol 10
2,4-Dichlorophenol 10
2,4-Dimeth y I phenol 10
2,4-Dinitrophenol 50
2,4-Dinitrotoluene 10
2,6-Dinitrotoluene 10
2-Chloronaphthalene 10
2-Chlorophenol 10
2-Me thy }naphthalene 10
2-Methylphenol 10
2-Nitrophenol 10
3&4-Methy I phenol 10
3,3 '-Dichlorobenzidine 20
4,6-Dinitro-2-methy I phenol 50
4-Bromophenyl phenyl ether 10
4-Chloro-3-methylphenol 20
4-Chlorophenyl phenyl ether 10
4-Nitrophenol 50
Acenaphthene 10
Acenaphthylene 10
Anthracene 10
Azobenzene 10*
Benz( a)anthracene 10
Benzidine 10*
Benzo(a)pyrene 10
Benzo(b )fluoranthene 10
Benzo(g,h,i)perylene 10
Benzo(k)fluoranthene 10
B is(2-chloroethoxy )methane 10
Bis(2-chloroethyl) ether 10
Bis(2-chloroisopropyl) ether 10
Bis(2-ethylhexyl) phthalate 10*
Butyl benzyl phthalate 10
Chrysene 10
Dibenz(a,h)anthracene 10
Diethy l phthalate 10
Dimethyl phthalate 10
Di-n-butyl phthalate 10
Di-n-octyl phthalate 10
Fluoranthene 10
Fluorene 10
E-4 Reporting Limit Evaluation
Parameter Permit-Specified RL
Hexachlorobenzene 10
Hexachlorobutadiene 10
Hexachlorocyclopentadiene 10
Hexachloroethane 10
Indeno( 1 ,2,3-cd)pyrene 10
Isophorone 10
Naphthalene 10
Nitrobenzene 10
N-Nitrosodimethylamine 10*
N-Nitrosodi-n-propylamine 10
N-Nitrosodiphenylamine 10
Pentachlorophenol 50
Phenanthrene 10
Phenol 10
Pyrene 10
Pyridine 10*
All analyses were reported to the required RLs unless noted in the text.
* Reporting limits for these analytes are not specified in either the Permit
or EPA Method 8270D. The reporting limits established by the laboratory
are reported here. The reporting limits are comparable to other analytes in
the same method.
E-5: Trip Blank Evaluation
All trip blanks for the 2014 sampling program were nondetect .
Blank . Sample Date Laboratory
1 81191201 4 Chemtech-Ford
E-6 Duplicate Sample Relative Percent Difference
Major Ions (mg/1) Cell 4A Tailings Fluid Cell65 RPD%
Carbonate <1 <1 NA
Bicarbonate <1 <1 NA
Calcium 445 406 9
Chloride 5900 5800 2
Fluoride 1290 1290 0
Magnesium 2990 2890 3
Nitrogen-Ammonia 2730 2780 2
Nitrogen-Nitrate 39.5 42.5 7
Potassium 724 644 12
Sodium 7190 6380 12
Sulfate 64900 65300 1
pH (s.u.) 1.7 1.7 0
TDS 97000 100000 3
Conductivity (umhos/cm) 73000 72800 0.3
Metals (ug/1)
Arsenic 70000 66900 5
Beryllium 190 188 1
Cadmium 1780 1630 9
Chromium 4620 4420 4
Cobalt 27500 23400 16
Copper 556000 491000 12
Iron 2280000 2280000 0
Lead 14800 12300 18
Manganese 120000 115000 4
Mercury 2.5 <2.0 NA
Molybdenum 40600 34800 15
Nickel 54100 48200 12
Selenium 2000 2240 11
Silver 197 222 12
Thallium 376 377 0.3
Tin <17000 <17000 NA
Uranium 159000 124000 25
Vanadium 535000 491000 9
Zinc 169000 137000 21
Radiologies (pCi/1)
Gross Alpha* 240000 166000 103.60
VOCS (ug!L)
Acetone <700 <700 NA
Benzene <5.0 <5.0 NA
Carbon tetrachloride <5.0 <5.0 NA
Chloroform <70.0 <70.0 NA
Chloromethane <30.0 <30.0 NA
MEK <4000 <4000 NA
E-6 Duplicate Sample Relative Percent Difference
Major Ions (mg/1) Cell 4A Tailings Fluid Cell65 RPD%
Methylene Chloride <5.0 <5.0 NA
Naphthalene <100 <100 NA
Tetrahydrofuran <46.0 <46.0 NA
Toluene <1000 <1000 NA
Xylenes <10000 <10000 NA
SVOCS (ug!L)
1,2,4-Trichlorobenzene <10 <10 NA
1,2-Dichlorobenzene <10 <10 NA
1 ,3-Dichlorobenzene <10 <10 NA
1 ,4-Dichlorobenzene <10 <10 NA
1-Methylnaphthalene <10 <10 NA
2,4,5-Trichlorophenol <10 <10 NA
2,4,6-Trichlorophenol <10 <10 NA
2,4-Dichlorophenol <10 <10 NA
2,4-Dimethylphenol <10 <10 NA
2,4-Dinitrophenol <20 <20 NA
2,4-Dinitrotoluene <10 <10 NA
2,6-Dinitrotoluene <10 <10 NA
2-Chloronaphthalene <10 <10 NA
2-Chlorophenol <10 <10 NA
2-Methylnaphthalene <10 <10 NA
2-Methylphenol <10 <10 NA
2-Nitrophenol <10 <10 NA
3&4-Methylphenol <10 <10 NA
3,3 '-Dichlorobenzidine <10 <10 NA
4,6-Dinitro-2-methylphenol <10 <10 NA
4-Bromophenyl phenyl ether <10 <10 NA
4-Chloro-3-methylphenol <10 <10 NA
4-Chlorophenyl phenyl ether <10 <10 NA
4-Nitrophenol <10 <10 NA
Acenaphthene <10 <10 NA
Acenaphthylene <10 <10 NA
Anthracene <10 <10 NA
Azobenzene <10 <10 NA
Benz(a)anthracene <10 <10 NA
Benzidine <10 <10 NA
Benzo(a)pyrene <10 <10 NA
Benzo(b )fluoranthene <10 <10 NA
Benzo(g,h,i)pery1ene <10 <10 NA
Benzo(k)fluoranthene <10 <10 NA
Bis(2-chloroethoxy)methane <10 <10 NA
Bis(2-chloroethy1) ether <10 <10 NA
Bis(2-chloroisopropyl) ether <10 <10 NA
E-6 Duplicate Sample Relative Percent Difference
Major Ions (mgll) Cell 4A Tailings Fluid Cell65 RPD%
Bis(2-ethylhexyl) phthalate <10 <10 NA
Butyl benzyl phthalate <10 <10 NA
Chrysene <10 <10 NA
Dibenz(a,h)anthracene <10 <10 NA
Diethy1 phthalate <10 <10 NA
Dimethyl phthalate <10 <10 NA
Di-n-butyl phthalate <10 <10 NA
Di-n-octyl phthalate <10 <10 NA
Fluoranthene <10 <10 NA
Fluorene <10 <10 NA
Hexachlorobenzene <10 <10 NA
Hexachlorobutadiene <10 <10 NA
Hexachl orocycl open tadi ene <10 <10 NA
Hexachloroethane <10 <10 NA
lndeno(l ,2,3-cd)pyrene <10 <10 NA
lsophorone <10 <10 NA
Naphthalene <10 <10 NA
Nitrobenzene <10 <10 NA
N-Nitrosodimethylarnine <10 <10 NA
N-Nitrosodi-n-propylamine <10 <10 NA
N-Nitrosodiphenylarnine <10 <10 NA
Pentachlorophenol <10 <10 NA
Phenanthrene <10 <10 NA
Phenol <10 <10 NA
Pyrene <10 <10 NA
Pyridine <10 <10 NA
Highlighted cells indicate an RPD that exceeded the 20% RPD criteria
Per the approved QAP, an RPD greater than 20% is acceptable if the reported results are less than 5 times the RL. These
results are provided for information only.
* Duplicate checks reported for gross alpha minus RN and U are not %RPD. Calculated values are based on the formula in
the approved QAP.
E-7 Radiologies Counting Error
Gros, ·Alpha
minu Rn & Counting
Gross Alpha U Precision Errer~ Within·
SainpJe ID minus Rh ·& w '(:tl 20% GW-QS GWQS
Cell1 331000 710 y 15 NA
Cell 2 Slimes 6890 98.1 y 15 NA
Cell3 19700 168 y 15 NA
Cell4A 240000 577 y 15 NA
Cell4ALDS 61800 289 y 15 NA
Cell4B 148000 446 y 15 NA
Cell 65 (Duplicate of
Cell4A) 166000 421 y 15 NA
GWQS = Groundwater Quality Standard
E-8: Laboratory Matrix QC
Matrix Spike % n~urCJ-y Comp;ui)ion
Lab Report SampleiD Analyte MS%REC
1408830 NIA Calcium* NC
1408830 NIA Sodium* NC
1408830 Cell4ALOS Calcium* NC
1408830 Cell4ALOS Chromium 69.8
1408830 Cell4A LOS Iron* NC
1408830 Cell4A LOS Sodium* NC
1408830 Cell4ALOS Tin 64.9
1408830 Ce114ALOS Zinc* NC
1408830 NIA Magnesium* NC
1408830 Cell4A LOS Magnesium* NC
1408830 Cell4A LOS Manganese* NC
1408830 Cell4ALOS Potassium* NC
1408830 Ce114ALOS Sulfate* NC
1408830 N/A Nitrate+Nitrite as N 77
1408830 Cell4ALOS Nitrate+ Nitrite as N 76
1408830 Cel14ALOS I ,2,4-Trichlorobenzene 34.4
1408830 Cel14ALOS Acenaphthene 47.6
1408830 Ceii4ALOS Alkalinity 0
NC = Not Calculated
*= Analyte concentration is too high for accurate matrix spike recovery and/or RPD.
N/A = QC was not performed on an EFRI sample.
Method Blank detections
Reported
Concentration
Lab Report Well/Sample Analyte (mg!L)
1408830 NA Iron 0.02
1408830 NA Calcium 0.03
1408830 NA Iron 0.001
1408830 NA Magnesium 0.01
1408830 NA Potassium 0.01
1408830 NA Sodium 0.03
1408830 NA Tin 0.008
1408830 NA Zinc 0.0001
1408830 NA Calcium 0.01
1408830 NA Magnesium 0.03
1408830 NA Manganese 0.002
1408830 NA Potassium 0.02
1408830 NA Sodium 0.1
1408830 NA Tin 0.002
1408830 NA Zinc 0.004
1408830 NA ' Ammonia as N 0.09
1408830 NA AmmoniaasN 0.1
LCSo/i R o <ccrJVcry
Lab Specified
Lab Report Analyte LCS %REC RECRange
1408830 1 ,2,4-Trichlorobenzene 41.2 44-142
MSD
%REC RECRange RPD
NC 70-130 NC
NC 70-130 NC
NC 70-130 NC
70.4 70-130 0.275
NC 70-130 NC
NC 70-130 NC
64.6 70-130 0.434
NC 70-130 NC
NC 70-130 NC
NC 70-130 NC
NC 70-130 NC
NC 70-130 NC
NC 90-110 NC
92 90-110 9.35
87 90-110 9.13
34.8 44-142 1.16
43.2 47-145 9.69
0 80-120 NC