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HomeMy WebLinkAboutDRC-2014-005081 - 0901a06880484d9dENERGYFUELS Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www.energyfuels.com August 29, 2014 VIA OVERNIGHT DELIVERY DRC-2014-005081 Mr. Rusty Lundberg Director of the Utah Division of Radiation Control State of Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144850 Salt Lake City, UT 84116-4850 Dear Mr. Lundberg: Re: State of Utah Radioactive Material License No. UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period January 1 through June 30,2014 As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65 (subpartl)), and License Condition 11.3A of State of Utah Radioactive Materials License No. UT 1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill for the period January 1, 2014 through June 30, 2014. If you have any questions regarding this report, please contact the undersigned at (303) 389- 4134. Yours very truly, ENERGY FUELS RESOURCES (USA) INC. Kathy Weinel Quality Assurance Manager cc: David C. Frydenlund Harold R. Roberts David E. Turk Frank Filas Jaime Massey August 29, 2014 VIA OVERNIGHT DELIVERY Mr. Rusty Lundberg Director of the Utah Division of Radiation Control State of Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144850 Salt Lake City, UT 84116-4850 Dear Mr. Lundberg: Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www .energyfuels.com Re: State of Utah Radioactive Material License No. UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effiuent Monitoring Report for Period January 1 through June 30, 2014 As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65 (subpart1)), and License Condition 11.3A of State of Utah Radioactive Materials License No. UT1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill for the period January 1, 2014 through June 30, 2014. If you have any questions regarding this report, please contact the undersigned at (303) 389- 4134. Yours very truly, {4)0ud_ ENERGY FUELS RESOURCES (USA) INC. Kathy Weinel Quality Assurance Manager cc: David C. Frydenlund Harold R. Roberts David E. Turk Frank Filas Jaime Massey White Mesa Uranium Mill Radioactive Materials License UT900479 Semi-Annual Effluent Monitoring Report (January through June 2014) Prepared For: Utah Department of Environmental Quality Division of Radiation Control Prepared by: Energy Fuels Resources (USA) Inc. 225 Union Boulevard, Suite 600 Lakewood, CO 80228 August 29, 2014 TABLE OF CONTENTS 1.0 INTRODUCTION .................................................................................................. 1 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING ..................................... 2 2.1 Program Overview .................... , .......................................................................... 2 2.2 Sampling Protocol and Analytical Results ............................................................ 2 2.3 General Observations ............................................................................................ 3 2.4 Site Specific Sampling Data ................................................................................. 4 2.5 Radon-222 ............................................................................................................ 6 3.0 EXTERNAL RADIATION (DIRECT GAMMA) .................................................. 7 4.0 VEGETATION SAMPLES ...................................................................................... 8 5.0 STACK SAMPLING ............................................................................................... 8 6.0 SURFACE WATER MONITORING .................................................................... 11 7.0 SOIL SAMPLING ................................................................................................. 11 8.0 METEOROLOGICAL MONITORING ..................... , .................................... , ....... 11 9.0 SIGNATURE ......................................................................................................... 12 LIST OF TABLES Table 1 NCRP Report 94-Global Pb-210 Concentration Example Table 2 Air Monitoring Station Results U-Nat (Comparison to Limits) Table 3 Air Monitoring Station Results Th-230 (Comparison to Limits) Table 4 Air Monitoring Station Results Ra-226 (Comparison to Limits) Table 5 Air Monitoring Station Results Pb-210 (Comparison to Limits) Table 6 Environmental OSL Dosimeter Measurements (Gamma) Table 7 Stack Sampling Requirements Table 8 Stack Effluent Concentrations and Release Rates l INDEX OF TABS A High Volume Air Monitoring Stations B BHV Air Sampling Graphs and Data Tables Tab 1 BHV -1 Air Sampling Graphs and Data Table Tab 2 BHV-2 Air Sampling Graphs and Data Table Tab 3 BHV-3 Air Sampling Graphs and Data Table Tab 4 BHV -4 Air Sampling Graphs and Data Table Tab 5 BHV -5 Air Sampling Graphs and Data Table Tab 6 BHV -6 Air Sampling Graphs and Data Table C BHV Air Sampling Laboratory Results and QA/QC D Air Particulate Loading Graphs and Supporting Data E Environmental Gamma (OSL) Dosimeter Graphs and Supporting Data F Vegetation Graphs, Data Table, Laboratory Results and QA/QC G Stack Sample Laboratory Results H Surface Water Graphs and Field Data Sheets I Soil Sample Graphs, Data Table, Laboratory Results and QA/QC ii WHITE MESA URANIUM MILL SEMI-ANNUAL EFFLUENT REPORT, JANUARY THROUGH JUNE 2014 1.0 INTRODUCTION The White Mesa Mill (the "Mill") has established monitoring programs to evaluate compliance with effluent limitations and to assess the potential for release of radioactive material into the local environment. These monitoring programs were developed and implemented at the time of Mill constmction, operated with appropriate adaptation over time, and are consistent with the Mill's State of Utah Radioactive Materials License No. UT1900479 (the "License") and guidelines developed by the United States Nuclear Regulatory Commission ("NRC") (NRC Regulatory Guide 4.14, Radiological Effluent and Environmental Monitoring at Uranium Mills-Rev. 1, ML003739941), 1980). Under these programs, the Mill monitors the following environmental media and conditions: a) Airborne particulate radionuclide concentrations obtained from the following sampling stations: • North, east and south of the Mill Site: BHV-1 and BHV-2 (north), BHV-5 (east), and BHV-4 (south). BHV-1 serves as a surrogate for the nearest resident (BHV -1 is approximately 1.2 miles north of the Mill, but approximately 0.4 miles closer to the Mill than the nearest resident); • A background location distant to and west of the Mill (BHV-3) that was monitored for airborne particulates up until November, 1995 (at which time background was established), which is no longer monitored for air particulates; and • A station specifically requested by the White Mesa Ute Community south of the Mill Site (BVH-6); b) External (direct) gamma radiation measured at air monitoring stations BHV -1, BHV-2, BHV-3, BHV-4, BHV-5 and BHV-6; c) Vegetation at three site periphery locations, for uptake of radionuclides; d) Stack release rates from the Mill's air emissions sources; e) Surface water at Cottonwood Creek and, when flowing, Westwater Creek, both located west of the Mill; f) Soil radionuclide activity obtained near the air particulate monitoring stations, during the third quarter of each year; 1 N:\WMM\Required Reports\Semi Annual Effluent Reports\2014 Jan-June\Jan_June_2014_SAER_text.docx g) Groundwater (up and down gradient) of the Mill facility; and 1 h) Seeps and springs in the vicinity of the Mill.1 This semi-annual effluent report provides the results of the specific monitoring and sampling activities that were undertaken during the subject reporting period. 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING 2.1 Program Overview The environmental airborne particulate monitoring program at the Mill utilizes four air sampling stations. Four high-volume continuous air sampling stations (BHV-1, BHV-2, BHV -4, and BHV -5) are required by the License. These sampling stations serve as sentinels for airborne particulate which could potentially emanate from the Mill site. In addition to its general site monitoring function, BHV -1 also serves as a conservative surrogate for concentrations at the nearest resident, because it is located approximately 1.2 miles north of the Mill just south of the nearest resident but between the Mill and that resident. With regard to background monitoring, the Mill previously operated a continuous high- volume air sampling station (BHV-3) which was located approximately 3.5 miles west of the Mill site. With the approval of NRC, this station (BHV-3) was removed from the active air monitoring program in November 1995. At that time, NRC determined that a sufficient air monitoring database had been compiled at BHV-3 to establish a representative airborne radionuclide background for the Mill. While air sampling was discontinued at this location, gamma measurements and soil sampling continue at BHV- 3. In addition to the environmental air sampling locations described above, an additional station (BHV-6) was installed at the request of the White Mesa Ute Community. This station began operation in July of 1999 and provides airborne particulate information in the southerly direction between the Mill and the White Mesa Ute Community. 2.2 Sampling Protocol and Analytical Results Airborne particulate monitors are operated continuously at each of the high-volume air sampling stations referenced above except BHV -3. Particulate sample collection filters are gathered by site technicians weekly in accordance with the Mill's environmental air sampling procedures and are composited on a quarterly basis for laboratory analyses. The collected filters are analyzed for Unat activity, Th-230 activity, Ra-226 activity, and Pb-210 activity. Fugitive dust standards for the facility are limited by the Mill's State of Utah Air Approval Order. The specific locations of the Mill's airborne particulate 1 Groundwater sampling and seeps and springs sampling are reported separately pursuant to the Mill's State of Utah Ground Water Discharge Permit No. UGW370004, and are not included with this report. 2 N:\WMM\Required Reports\Semi Annual Effluent Reports\2014 Jan-June\Jan_June_2014_SAER_text.docx monitoring stations are depicted on the figure entitled High Volume Air Monitoring Stations included as Attachment A. Station BHV-3, which is no longer sampled for air particulates, is located approximately 3.5 miles west of the Mill facility and is not shown on the Figure. The analytical results of radionuclide particulate sampling for each monitoring station operated during this reporting period are provided in Attachment B under separate sampling station attachment tabs (Tabs 1-6). Each tab contains graphical illustrations of the radionuclide concentrations in log-scale presentation format. The graphs display reported data over time since the 1981 inception of the Mill's environmental air particulate monitoring program. The actual analytical results (and associated QA/QC information) reported by the laboratory for the reporting period are provided under Attachment C. In addition to the analyses for radionuclides, particulate loading is determined for each filter and composited as a quarterly mass-loading estimate for review purposes only. Graphs showing particulate loading at each station and the underlying data are included as Attachment D. The first 2 sampling periods of 2012 have been omitted from particulate loading on the graph for BHV -6 in Attachment D. The timer on the airborne particulate monitoring station at BHV -6 malfunctioned, and the data are considered invalid due to the inability to measure the time sampled. The timer was replaced prior to the third sampling period in 2012 and all other measurements are valid. For graphical jJJu tration purposes, values reported at zero, values reported at less than the prescribed detection limit < J x J0-1G uCi/ml), and missing values were plotted as 1 x 10-16 uCi/ml concentrations. Where other "less than" values were indicated (i.e., where detection limits for the data varied from 1 X 10'16 uCi/ml), the detection limit concentration was utilized for plotting the data point. This graphing convention is not utilized to formulate station average information, nor is it intended as a precedent for data treatment. Rather, the intent is to provide a conservative viewable depiction of site airborne radionuclide information. This is considered to be a conservative approach, because the actual concentration below the detection limit cannot be determined and, as a result, the plotted point will be at the same or a higher concentration than the actual activity concentration of the collected sample. 2.3 General Observations The results of environmental air monitoring for this semi-annual period indicate that for all radionuclides at all monitoring stations, airborne radionuclide particulate activity concentrations were well below regulatory Effluent Concentration Limits ("ECL's") and the Mill's ALARA goals, which are set at 25% of the ECLs. It is noteworthy and expected that Pb-210 concentrations are elevated when compared to the other parent radionuclide concentrations (i.e. U-nat, Th-230 and Ra-226). This phenomenon is due to the well-established controlling effect experienced worldwide as a 3 N:\WMM\Required Reports\Semi Annual Effluent Reports\2014 Jan-June\Jan__June_2014_SAER_text.docx result of the ubiquitous presence of radon in the eruth's atmosphere. Accordingly, the elevated Pb-210 presence in disequilibrium with parent radionuchdes measured here is not associated with uranium milling operations. Rn-222 emanates as a decay-chain progeny of the Ra-226 contained in the soil of the earth's crust and is dispersed generally throughout the earth's atmosphere. The electrically charged short and long-lived decay products of Rn-222 attach to ambient dust particles found naturally in the atmosphere and are carried with the air. Pb-210 is the longest lived of these decay products and is the decay product of the shorter-lived radon progeny. As such, it accumulates as an electrical attachment on the natural ambient dust in the atmosphere and is generally measured at elevated activity when compared to local decay-chain parent radionuclide activity, regardless of uranium milling activity. At the Mill's BHV air monitoring stations, all dust (ambient natural and mill derived) is collected by the sample filter. Because of the natural elevation of Pb-210 accumulated as an attachment to the naturally occurring ambient dust particles collected by the air sampling equipment, Pb-210 is commonly elevated and in disequilibrium when compared to parent radionuclide activity, regardless of the Mill's presence. By way of illustration, average ground-level concentrations have been reported for selected States (NCRP Report 94, 1992) and are summarized in Table 1 below, demonstrating that elevated Pb-210 activity is present where no uranium milling operations are located nearby. In April 1977, prior to Mill construction and Mill operations, air farticulate Pb-210 was measured at the Mill site to be 1.3E-14 uCi/rnl (13.0E-3 pCi/m )2. Table 1-NCRP Report 94-Global Pb-210 Concentration Example ·State Pb-210 Concentration uBq/M3 uCi/ml California 600 1.6E-14 Illinois 1500 4.1E-14 Ohio 300 8.1E-15 Massachusetts 700 1.9E-14 2.4 Site Specific Sampling Data The results of airborne particulate monitoring for the period (without background subtraction) are provided by sampling station and radionuclide in Tables 2 through 5 below. Along with these data, the tables present comparative ECL's and the ECL percentage measured at each of the monitoring stations sampled during the period. A review of these data support the conclusion that airborne particulates are well controlled at the Mill. In all cases, the measured activity concentrations were well within the ECL, as well as the Mill's ALARA goal (i.e. 25% of the ECL). Lower Limits of Detection consistent with NRC Regulatory Guide 4.14 were maintained by the Mill's contract analytical laboratory for this reporting period. 2 See the Environmental Report, White Mesa Uranium Project, San Juan County, Utah for Energy Fuels Nuclear, Inc. prepared by Dames & Moore, January 30, 1978, Section 2.9.1.1 4 N:\WMM\Required Reports\Semi Annual Effluent Reports\2014 Jan-June\.Jan_June_2014_SAER_text.docx The data obtained since program inception in 1981 indicates that only one individual quarterly measurement (Th-230 at BHV-5 for the 2nd Quarter of 1996) has ever exceeded the ECL at the Mill. While it is important to consider and evaluate an individual measurement exceeding the ECL, it is the average annual concentration that is of primary significance for public dose estimation purposes. In that instance, the average annual concentration of Th-230 for BHV-5 in 1996 was well below the ECL. Data obtained since program inception in 1981 also indicate that, with very few exceptions, the gross (background inclusive) measurements do not exceed the site's ALARA goal (i.e. only nine of the several thousand total gross radionuclide determinations to date exceeded the Mill's self-imposed 25% ALARA goal). Table 2-Air Monitoring Station Results U-Nat (Comparison to Limits) 1st and 2nd Quarters 2014 Monitoring 1st Qtr. 2nd Qtr. Effluent Average Station Result Result Concentration Percent (uCilrnl) (uCilrnl) Limit (ECL) ECL (uCilrnl) BHV1 1.07E-15 2.24E-15 9.00E-14 1.84E+00 BHV2 4.63E-16 3.04E-16 9.00E-14 4.26E-01 BHV4 4.69E-15 4.16E-15 9.00E-14 4.92E+00 BHV5 4.74E-15 8.18E-15 9.00E-14 7.18E+00 BHV6 8.92E-15 8.29E-15 9.00E-14 9.56E+00 Table 3-Air Monitoring Station Results Th-230 (Comparison to Limits) 1st and 2nd Quarters 2014 Monitoring 1st Qtr. 2nd Qtr. Effluent Average -" Station Result Result Concentration Percent (uCilrnl) (uCilrnl) Limit (ECL) ECL (uCilrnl) I BHV1 2.07E-16 5.14E-16 2.00E-14 1.80E+00 BHV2 4.97E-17 7.92E-17 2.00E-14 3.22E-01 BHV4 1.37E-16 6.96E-16 2.00E-14 2.08E+00 BHV5 1.42E-15 1.34E-15 2.00E-14 6.90E+00 BHV6 7.68E-16 5.35E-16 2.00E-14 3.26E+00 5 N:\WMM\Required Reports\Semi Annual Effluent Reports\2014 Jan-June\Jan_June_2014_SAER_text.docx Table 4-Air Monitoring Station Results Ra-226 (Comparison to Limits) 1st and 2"d Quarters 2014 Monitoring 1st Qtr. 2nd Qtr. Effluent= Average Station Result Result Concentration Percent (uCilml) (uCilml) Limit (ECL) ECL (uCi/ml) BHVl 3.69E-16 1.09E-15 9.00E-13 8.11E-02 BHV2 1.15E-16 1.82E-16 9.00E-13 1.65E-02 BHV4 3.53E-16 1.77E-15 9.00E-13 1.18E-01 BHV5 3.48E-15 1.76E-15 9.00E-13 2.91E-Ol BHV6 1.50E-15 6.72E-16 9.00E-13 1.21E-01 Table 5-Air Monitoring Station Results Pb-210 (Comparison to Limits) 1st and 2"d Quarters 2014 Monitoring 1st Qtr. 2nd Qtr. Effluent Average Station Result Result Concentration Percent (uCi/ml) (uCi/ml) Limit (ECL) ECL -~~ (uCilml) BHVl 1.24E-14 1.23E-14 6.00E-13 2.06E+00 BHV2 1.49E-14 1.21E-14 6.00E-13 2.25E+00 BHV4 1.08E-14 1.06E-14 6.00E-13 1.78E+00 BHV5 1.50E-14 1.42E-14 6.00E-13 2.43E+00 BHV6 1.61E-14 1.20E-14 6.00E-13 2.34E+00 2.5 Radon-222 Due to the unavailability of monitoring equipment to detect the revised 10 CFR Part 20 standard, and with the approval of the NRC, Radon 222 monitoring at BHV stations was discontinued in 1995. Instead, compliance with these limits and the requirements of R313-15-301 is demonstrated by a calculation, authorized by the NRC and as contemplated by R313-15-302(2)(a). A copy of the Technical Evaluation Report evidencing such approval was enclosed with correspondence to the Division of Radiation Control ("DRC") on July 28, 2008. This calculation is performed by use of the MILDOS code for estimating environmental radiation doses for uranium recovery operations (Strenge and Bender 1981) and more recently in 2003 by use of the updated MILDOS AREA code (Argonne 1998). The analysis under both the MILDOS and MILD OS AREA codes assumes the Mill to be processing high grade Arizona Strip ores at full capacity, and calculates the concentrations of radioactive dust and radon at individual receptor locations around the Mill. 6 N:\WMM\Required Reports\Semi Annual Effluent Reports\2014 Jan-June\Jan_June_2014_SAER_text.docx The MILDOS and MILDOS AREA codes calculate the combined Total Effective Dose Equivalent ("TEDE") from all relevant pathways, including both air particulate and radon, at a number of locations including the nearest residence (the individual likely to receive the highest dose from the licensed operation), approximately 1.6 miles north of the Mill. These calculations reveal projected doses to the individual likely to receive the highest dose from the licensed operations to be well below the 100 mrem regulatory limit in R313-15-301(1)(a) for all pathways, including air particulate and radon, and well below the ALARA goal of 10 mrernlyr for air emissions excluding radon as set out in R313-15-101(4). MILDOS AREA modeling was recently conducted in support of the Mill's 2007 License Renewal Application, utilizing the MILDOS-AREA code (Version 2.20~), to estimate the dose commitments at various receptor locations for processing of Colorado Plateau ore (0.25% U30 8 and 1.5% V20 5) and Arizona Strip ore (0.637% U30 8). The process rate was assumed to be at full capacity of 730,000 tons per year (an average of 2,000 tons per day) with an average uranium recovery yield of 94%. That modeling showed a TEDE of 2 mrem per year at the nearest resident (3 mrem per year at the nearest potential residence, being the location of BHV -1 at the northern property boundary of the Mill site), which included the dose from all radionuclide sources, including radon. The modeled dose from radon itself was therefore a fraction of the TEDE and well within the regulatory limits. 3.0 EXTERNAL RADIATION (DIRECT GAMMA) Gamma exposure rate estimates were measured for the reporting period utilizing optically stimulated luminescence dosimeters ("OSLs"). These dosimeters were located at each of the Mill's high-volume air sampling stations (BHV-1, BHV-2, BHV-4, BHV-5 and BHV-6) and at the designated background monitoring station (BHV-3). Measurements obtained from location BHV-3 have been designated as background due to BHV-3's remoteness from the Mill site (i.e., BHV-3 is located approximately 3.5 miles west of the Mill site). The results of the environmental OSL measurements and semi-annual cumulative above-background data are provided in Table 6 below. In addition, measurement data obtained at these locations are graphically presented in Attachment E to this report. 7 N:\WMM\Required Reports\Semi Annual Effluent Reports\2014 Jan-June\Jan_June_2014_SAER_text.docx Table 6-Environmental Optically Stimulated Luminescence Dosimeter ~easurements((;amma) ' Monitoring 1st Qtr 2nd Qtr 1st Qtr 2nd Qtr Cumulative Station Result Result Result Less Result Less Semi- (mrem) (mrem) Background Background Annual (mrem) (mrem) Estimate (mrem) BHV1 32.0 37.7 3.9 4.1 8.0 BHV2 28.9 30.8 0.8 0.0 0.8 BHV3 28.1 33.6 0.0 0.0 0.0 BHV4 31.5 32.0 3.4 0.0 3.4 BHVS 32.6 37.2 4.5 3.6 8.1 BHV6 33.2 31.1 5.1 0.0 5.1 The results for this period indicate that above background measurements for stations BHV-1, BHV-2, BHV-4, BHV-5 and BHV-6 are within regulatory limits. BHV-1 is at the location of the nearest potential residence. The nearest actual residence is approximately 0.4 miles north of BHV-1. The annual limit for an individual member of the public is 100 mrem/yr for combined internal and external exposure. 4.0 VE<;ETATION SA~PLES Vegetation samples are collected at three locations around the Mill property. The sampling locations are: 1) northeast, 2) northwest and 3) southwest of the Mill facility. The NRC Regulatory Guide 4.14 requires that three samples be collected during the grazing season, without specifying exact months or times during the season. During the 2014 grazing season, two sets of samples were collected on April 16, 2014 and June 10, 2014. A third set of samples is planned for the fall season. The data from the fall season sampling will be included in the July through December 2015 Semi-Annual Effluent Report ("SAER") which will be submitted to the DRC on March 1, 2015. Data from the April and June sampling events are included in this report. Graphical log-scale presentation of the vegetation sampling results, together with the analytical results reported by the Mill's contract laboratory (including QA/QC information) for this sampling period, are included as Attachment F of this report. The 2014 data results are within the variation of previous sampling episodes. 5.0 STACK SA~PLIN(; Under Section 5.0 of Tab 1.4 of the Mill's Environmental Protection Manual, Revision: EFR-3, 12/12 (the "Environmental Protection Manual") gas stack samples are collected at the Mill in accordance with the calendar year schedule shown below: 8 N:\WMM\Required Reports\Semi Annual Effluent Reports\2014 Jan-June\Jan_June_2014_SAER_text.docx Table 7 -Stack Sampling Requirements Frequency Feed Stack (Grizzly Stack for Packaging Baghouse) Yellowcake Dryer (Yellowcake Baghouse) Quarterly None If operating, U-nat If operating, U-nat Semi-annually If operating, U-nat, If operating, U-nat, If operating, U-nat, Th-230 Th-230, Ra-226, Pb-Th-230, Ra-226, 210 Pb-210 The analytical results of stack sampling conducted for the 1st and 2nd quarters of 2014, as well as for the 3rd and 4th quarters of 2013, are provided in Table 8 below, indicating the uCi/cc concentration in the stack emissions and the stack's radionuclide release rate (uCi/sec) for U-Nat, Th-230, and Ra-226 at each of the stacks sampled. The Pb-210 results are discussed below. The actual analytical results reported by the laboratory for the 1st and 2nd quarters of 2014 are provided in Attachment G to this report. As shown on Table 8, the laboratory did not report the Pb-210 data for the 2nd quarter of 2014. The tracer yield for the samples was too low and insufficient for completion of the analyses. The entire sample volume was consumed during the initial analysis and there was no opportunity for reanalysis. EFRI was not notified of the issue by the laboratory until August of 2014, and therefore, could not recollect the samples. EFRI is exploring other laboratory options to prevent reoccurrence of data loss in the future. The south yellowcake dryer, yellowcake baghouse, and grizzly baghouse operated during the 1st and 2nd quarters of 2014. The north yellowcake dryer has not been in operation since the 3rd quarter of 2012, and therefore, has not been sampled since it was last in operation. It is also important to note that stack effluent concentrations are not comparable to environmental air sampling station ECL's for regulatory compliance purposes. The ECL is a limit that applies to the receptor locations and is not applicable to effluents from mill processes on the Mill site. These stack release data are more appropriately utilized for dose modeling purposes, and dose modeling is not computed for semi-annual reporting purposes. 9 N:\WMM\Required Reports\Semi Annual Effluent Reports\2014 Jan-June\Jan_June_2014_SAER_text.docx Table 8-Stack Effluent Concentrations and Release Rates U-Nat U-Nat. Th-230 Th-230 Ra-226 Ra-226 u/Ci/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec I 3nl Qtr, 2013* ' South YC Not Not Not Not Dryer, Run 1 3.89E-10 2.50E-04 Reguired Required Rt~guired Reguired South YC Not Not Not Not Dryer, Run 2 4.86E-10 2.82E-04 Required Required Reg_uired R~uired Yellowcake Not Not Not Not Baghouse 1.04E-08 1.73E-02 Required Required Required Required 4th Qtr, 2013* c • South YC Dryer, Run 1 2.70E-10 1.66E-04 2.33E-14 1.43E-08 7.77E-15 4.76E-09 South YC Dryer, Run 2 2.66E-10 1.65E-04 1.48E-13 9.13E-08 2.35E-14 1.46E-08 Yellowcake Baghouse 8.91E-09 1.55E-02 1.67E-11 2.91E-05 4.60E-13 S.OlE-07 Grizzly Not in Not in Not in Not in Not Not Baghouse** operation operation operation operation Rf~guired Rt~guired 1st Qtr 2014* South YC Not Not Not Not Dryer, Run 1 2.53E-10 1.65E-04 R!<quired Re__quired" Reg_uired Rf~guired South YC Not Not Not Not Dryer, Run 2 2.45E-10 1.67E-04 Re_quired Required Reg_uired Rf~guired Yellowcake Not Not Not Not Baghouse 9.87E-10 1.83E-03 Required Required Required Required 2"d Qtr, 2014* I~ South YC Dryer, Run 1 1.79E-09 1.04E-03 2.22E-14 1.29E-08 3.40E-14 1.97E-08 South YC Dryer, Run 2 2.19E-12 1.25E-06 3.25E-14 1.86E-08 3.44E-14 1.97E-08 Yellowcake Baghouse 8.48E-10 1.25E-03 2.82E-13 4.17E-07 2.11E-13 3.11E-07 Grizzly I I Not Not Baghouse 9.10E-12 6.40E-06 2.04E-12 1.43E-06 Required Required *The North Yellowcake Dryer was not in operation during 2013 or the first half of 2014 .. **The Grizzly Baghouse was not in operations during the 3rd and 41h quarters of 2013. 10 N:\WMM\Required Reports\Semi Annual Effluent Reports\2014 Jan-June\Jan_June_2014_SAER_text.docx Pb-210 Pb-210 uCi!cc uCi/sec Not Not Reg_uired Required Not Not Reg_uired Required Not Not Req~ired Required 2.11E-13 1.29E-07 1.65E-13 1.02E-07 1.16E-12 2.03E-06 Not Not R~guired Required Not Not Rf~guired Required Not Not Re_guired Required Not Not Reqpired Required No data reported. See Section 5.0 above for details. Not Not Required Required I 6.0 SURFACE WATER MONITORING Under the License, Part 11.2 B surface water samples are required to be obtained annually from Westwater Canyon and semi-annually from Cottonwood Creek. Sediment samples from Westwater Canyon are taken in place of the Westwater Canyon surface water sample where surface water is not available for sampling. Westwater Canyon surface water was not sampled in the first or second quarter of 2014, because no water was present during this reporting period. Attempts to collect a surface water sample from Westwater Canyon will continue through the next reporting period. If no surface water is available, a sediment sample will be collected as required. The Mill's Environmental Protection Manual requires that samples from Cottonwood Creek be analyzed for TDS and total suspended solids ("TSS") quarterly, and the License, Part 11.2 B requires that samples from Cottonwood Creek be analyzed for dissolved and suspended radionuclides including Gross Alpha, U-nat, Ra-226, and Th- 230 semi-annually. In accordance with these requirements, Cottonwood Creek was sampled for TDS and TSS during the 1st quarter, and was sampled for TDS, TSS, and the radionuclides during the 2nd quarter. The field data sheets for the surface water sampling events, along with graphs showing historic results are included as Attachment H. The results of this sampling indicate that surface water concentrations remain low and within the range of typical background levels. 7.0 SOIL SAMPLING Under Tab 4.1 of the Mill's Environmental Protection Manual, surface soils are required to be sampled at the Mill's air monitoring stations (BHV-1, BHV-2, BHV-3, BHV-4, BHV-5 and BHV-6) once per year during August or as soon as possible thereafter, but no later than September 30 of each year. In accordance with the Mill's Environmental Protection Manual, surface soils will be collected during the third quarter of 2014 and will be discussed in the July through December 2014 report. 8.0 METEOROLOGICAL MONITORING As in prior reporting periods, an independent contractor has prepared the White Mesa Mill Semi-annual Meteorological Monitoring Report for the period of January through June 2014. This information is retained at the Mill site for agency review. 11 N:\WMM\Required Reports\Semi Annual Effluent Reports\2014 Jan-Juue\Jan_June_2014_SAER_text.docx 9.0 SIGNATURE This report was prepared by Energy Fuels Resources (USA) Inc. on August 29, 2014. Energy Fuels Resources (USA) Inc. Frank Filas Vice President, Permitting and Environmental Affairs 12 N:\WMM\Required Reports\Semi Annual Effluent Reports\2014 Jan-June\Jan_June_2014_SAER_text.docx ATTACHMENT A HIGH VOLUME AIR MONITORING STATIONS U1 I* I I __ ..,_ __________ ----+----- I . ~ ~ I , ~ , I ; ~ ...... r . 1 *'..... ,-.J I I .... ,,,~. ' I'Y ,' I I ~ i . ,,1 ,~.. i -+------------~-t----:-1-1----:.----1 ., , : I r' ' , ·~I , . .. , i l\1\\1 .J I " ' , ~ I ,~ \ ,,,' I ' ' . l ._. I 1 I i 'It I I ~ • , : ,, . , ~-I ... I ! I •• • I -= --t-~-----------~'t.. 1 -t '~ : I I "•4 ) -~ I t. : ~ ~~l \ I / ' ,. : ( I ~ ~ ) ' ; : ('-' . ... -' .. --~ l ,,_, io / .... ~ :I .. .. .. ~ 0 ' I I -------r·--- ' I ' -r --------J I 1 I I I N I I I ~~ 1\ I J i I I I I I I -·-·• •• ·---2 I " _____ ,_ /, I - ' . I I ' \ I I . I , 0 2000 2000 , I b-CiJW ', SCAl£ II FEET ~--';f'I-1---I - 12 ' • • ------f-- a I .,~ i I .,., • I ~ .. ,, .... J\': : ., ...... • -'. 1 ~, ~"0 ( 1 '~~,-'' ... J,'_... \ I · ~...--'I -.------~,--· ----~-. ;,_.-~----E [ I '"'· I ,_,,,, ~-'' -I ! I -! 1 't?nf"-deHv-s 0 f---~-t{_. __ ... -----i-----~~--~ . \~ . . - ''\ I ,/-, I I ' • ,' ·1 ' '·I· .. . .. ~ .. ./ '~ , .. 't---'( ~ I ~ ' I ' I ., .. I \ • ----.;....~-----.. ---1 t' • •• I I ~ \ ( : , , I ' t'' I ( .. I • ' • I : ,./ I I · ;,. o . BHV· I ----.,.-··-- BIW-6 : : • • I __________ J_Lt ___ J ! ________ __\ _______________ ..... I • \ -I I I ' ., 1/ L I : ~·~ . ! -; ............ ., I L_ __ ~ \ I . • I . I \ . 4: ~­~r -J : -~ ...1 \ ... 4 ~----l-----~-·-----. ---~i __ -' ·--------------------------~ ~,· _., .. \i : l I ', I ~, I \ ' ,.... ' ' .-" ....._, I ' I '--- • • -• ' 1 -, t ( f'' ~11 ,._~ ,.~· ~ \ .. , "' i ~ I I • 1 n~Y -J t-7-L-------:,.,.... -~It,--. -------~---_____/b_ ---- _ ........ Property Boundary Reservation Boundary Canyon Rim 0 Air Monitor Stations •· \ .. • I -,-:I. 4 l \. \~ .,. . -\, \lt.. C:.l i _, ~.. ~ ~~ ·. I --o y,~). !S ~ ~~\,. I..(. f """" . l I • .., ' l -o • -. --. --~ --~~~~---_._--o---_ _. ---------~.~ I 6 -:. . .,.. ' *"' .. ~~~,,· *'f, ' .. • "\ J ..A •..._ -I , .. , ~ , '~... ~ ll'~ ( ·l"' ' ~....... .. '!...., .. # .... :·. ##\· ' ~. ~. . :,( ~, ~ l • ·--·-··--·---· ·4--~ "i ---~,:~---.-­~ --... ~ .. , '~ ..... . ~ '·~ .l i ~ . \ I ·#~,, I , .. ~ ~, ,, • ....., ..... ._ ... (USA) lllc. ,.... WHITE MESA MILL ...,..... ur g,. , .. -.. WIIM -_,---.... &3-,_.. ....... ---- ATTACHMENT B BHV AIR SAMPLING GRAPHS AND DATA TABLES TAB 1 BHV -1 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-1U Effluent Concentration Limit = 2E-14 uCi/ml BHV-lT Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit= 6E-13 uCi/ml BHV-1PB ALARAGoal = 2.25E-14 uCi/ml ALARA Goal-·SE-13 uCi/ml ALARAGoal = 2.25E·13 uCi/ml ALARA Goal-1.5E-13 uCi/ml Pr!!-i9!l4 MPc Umlt ~ SE-12 uCi/ml Pre 1994 MPC Limit= SE-14 uCi/ml Pre 1.9!111 MPC Umlt"' 2E-12 uCi/ml Pre 1994 MPC Limit-4E-12 uCi/ml Pre 1994 A LARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL= .SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone ~FC EFCA 9/28/1981 2.35E-15 5.00E-12 1.25E-12 7.82E·16 8.00E-14 2.00E·14 1.06E-15 2.00E-12 5.00E-13 2.57E-14 4.00E-12 1.00E-12 12/14/1981 1.56E-15 5.00E-12 1.25E-12 1.49E-15 8.00E-14 l.OOE-14 '1.93E-15 2.00E-12 5.00E-13 2.64E-14 4.00E-12 1.00E-12 ?/29/1982 2.16E-15 S,OOE-12 1.25E-12 2,93E-15 8.00E-14 2.00E·14 1.16E-15 2.00E-12 S.OOf-13 2.09E-14 4.00E-12 l.OOE-12 j 6/30/1982 .4..69E-15 S.OOE-12 1.25E-12 3.46E-15 8.00E-14 .2.00E·14 2.38E-15 2.00E-12 $.01*13 2.14E-14 4.00E-12 l.OOE-12 9/27/1982 4.45E-15 S.OOE-12 1.25E-12 3.29E·15 8.00E-14 2.00E·14 3.23E-15 2.00E·12 5.00E-13 1.99E-14 4 OOE-12 l.OOE-12 I 1/3/1983 4.39E-15 S.OOE-12 1.25E-12 5.91E·16 8.00E-14 2.00E-14 9.14E-16 2.00E-12 5.00E-13 4.87E-14 4.00E-12 l.OOE-12 4/4/1983 7.51E-16 5.00E-12 1.25E-12 2.13E-16 8.00E-14 2.00E-14 3.20E-16 2.00E-12 5.00E-13 L88E-14 4.00E-12 l.OOE-12 9}30/1983' 2.68E-16 5.00E-12 1.25E-12 6.92E-16 S.OOE-14 2.00E·14 7.92E-16 2.00E-12 5.00E-13 2.00E-14 4.00E-12 l.OOE-12 ! 10/3/1983 5.00E-12 1.25E-12 S.OOE-14 2.00E-14 O.OOE+OO 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 1 1/3/1984 2.87E-15 5.00E-12 1.25E-12 1.14E·16 8.00E-14 2.00E-14 1.79E-16 2.00E-12 5.00E-13 1.06E-14 4.00E-12 l.OOE-12 4/2/1984 1.59E-15 S.OOE-12 1.25E-12 3.40E·16 S.OOE-14 2.00E-14 3.71E-16 2.00E·12 5.00E-13 3.34E-14 4.00E-12 l.OOE-12 I 7{1;{'1!(}84 3.10E-15 S.OOE-12 1.25E-12 l.OOE-15 S.OOE-14 2.00E-14 2.09E-15 2.00E-12 S.OOE-13 l.SSE-14 4.00E-12 1.00E-12 I 10/1/1984 6.42E-16 S.OOE-12 1.25E-12 1.39E-16 8.00E-14 2.00E-14 1.94E-16 2.00E-12 5.00E-13 1.85E-14 4.00E-12 l.OOE-12 1/2/1985 5.06E-16 S.OOE-12 1.25E-12 4.56E-16 S.OOE-14 2.00E-14 3.49E-16 2.00E-12 5.00E-13 3.03E-14 4.00E·12 l.OOE-12 4}1/1985 O.OOE+OO S.OOE-12 1.25E-12 1.23E-15 8.00E-14 2.00E-14 4.88E-16 'l.OOE-12 S.OOE-13 1!.06E·15 4.00E-12 1.00E-12 7/l/1985 7.17E-16 5.00E-12 1.25E-12 8.00E-14 2.00E-14 1.05E-15 2.00E-12 5.00E-13 1.15E·14 4.00E-12 l.OOE-12 9)30/1985 6.13E-16 5.00E-12 1.25E-12 1.18E·16 8,00E-14 2.00E-14 3.71E-16 2.00E-12 S.OOE-13 3.64E-15 4.00E·12 l.OOE-12 1/2/1986 3.42E-15 5.00E-12 1,25E-12 4.74E·16 8.00E-14 2.00E-14 2.00E·12 5.00E-13 4.00E-12 1.00E-12 4/1/1986 3.98E-15 S.OOE-12 1.25E-12 9.74E-16 8.00E-14 2.00E·14 1.50E-15 2.00E-12 S.OOE-13 1.41E-14 4.00E-12 l.OOE-12 6/30/1986 5.51E-17 5.00E-12 1.25E-12 3.52E·16 8.00E-14 2.00E-14 1.37E-15 2.00E·12 5.00E-13 1.23E-14 4.00E-12 l.OOE-12 10/27/1986 1.99E-15 5.00E-12 1.25E-12 3.06E-16 8.00E-14 2.00E-14 1.25E-15 2.00E-12 S.OOE-13 1.08E-14 4.00E-12 l.OOE-12 12/15/1986 1.67E-15 5.00E-12 1.25E-12 1.16E·16 8.00E-14 LOOE-14 5.98E-16 2.00E·12 5.00E-13 1.37E-14 4.00E-12 l.OOE-12 3/16/1987 2.33E-15 5.00E-12 1.25E-12 4.30E-16 8.00E-14 2.00E-14 1.92E-16 2.00E-12 S.OOE-13 5.59E-14 4.00E-12 1.00E-12 5/11/1987 2.36E-15 5.00E-12 1.25E-12 7.69E·16 8.00E-14 2.00E-14 8 76E-16 2.00E·12 S.OOE-13 1.45E-14 4.00E-12 l.OOE-12 9/9/1987 2.27E-15 5.00E-12 1.25E-12 2.44E-15 8.00E-14 2.00E-14 8.51E-16 2.00E-12 S.OOE-13 3.14E-14 4.00E-12 l.OOE-12 ll/i/ll87 2.75E-15 S.OOE-12 1.25E-12 2.46E·15 8.00E·14 2.00E-14 1.34E-15 2.00E·12 5.00E-13 2.79E-14 4.00E-12 l.OOE-12 2/16/1988 1.07E-15 S.OOE-12 1.25E-12 1.47E·16 S.OOE-14 2.00E-14 4.44E-16 2.00E-12 5.00E-13 4.01E-14 4.00E·12 1.00E-12 5/18/1988 1.98E-15 :;,OOE-12 1.25E-12 1.25E-15 S.OOE-14 2.00E-14 6.40E-16 2.00E-12 5.00E-13 1.07E-14 4.00E-12 1.00E-12 8/15/1988 2.06E-15 S.OOE-12 1.25E·12 3.41E-15 S.OOE-14 2.00E-14 5.08E-16 2.00E-12 5,00E-13 1.62E-14 4,00E-12 1.00E-12 ll/.14/1988 3,94E-15 -5.00E-12 1.25E-12 2.12E-15 S.OOE-14 2.00E-14 1.01E-15 2.00E-12 S.OOE-13 2.47E-14 4.00E-12 1,00E-12 2/13/1989 1.99E-15 S.OOE-12 1.25E-12 5.73E·16 8.00E-14 2,00E-14 5.99E-16 2.00E·12 5.00E-13 3.23E-14 4.00E-12 l.OOE-12 5/15/1989 1.70E-15 S.OOE-12 1.25E-12 6.32E·16 8.00E-14 2.00E-14 5.86E-16 2.00E-12 5.00E-13 6.16E-15 4.00E-12 1 OOE-12 8/14/1989 2.31E-15 5.00E-12 1.25E-12 2.31E·16 S,OOE-14 2.00E-14 1.77E-16 2.00E-12 S.OOE-13 7.65E-15 4.00E-12 l.OOE-12 ll/13/1989 4.72E-15 5.00E-12 1.25E-12 1.71E-15 S.OOE-14 2.00E-14 1.52E-15 ~.OOE-12 S.OOE-13 1.89E-14 4.00E-12 1.00E-12 2/12/1990 3.44E-16 S.OOE-12 1.25E-12 8.39E-16 S.OOE-14 2.00E-14 8.31E-16 2.00E-12 S.OOE-13 2.57E-14 4.00E-12 l.OOE-12 5/14/1990 3.03E-15 S.OOE-12 1.25E-12 1.47E·15 S.OOE-14 .2 OOE-14 1.04E-15 2.00E·12 5.00E·13 1.79E-14 4.00E-12 1.00E-12 8/13/1990 1.64E-15 5.00E-12 1.25E-12 1.49E-15 8.00E-14 2.00E-14 3.34E-16 2.00E-12 5.00E-13 8.27E-15 4.00E-12 l,OOE-12 11/12/1990 1.48E-15 5.00E-12 1.25E-12 7.50E-16 S.OOE-14 2.00E-14 5.80E-16 2.00E-12 5.00E-13 2.16E-14 4.00E-12 l.OOE-12 ,2/11/1991 1.90E-16 5.00E·12 1.25E-12 3.48E-17 S.OOE-14 2.00E·14 7.91E·17 2.00E-12 S.OOE-13 3.79E-14 4.00E-12 l.OOE-12 5/13/1991 3.42E-16 5.00E-12 1.25E-12 1.34E·15 8.00E-14 2.00E-14 7.39E-16 2.00E·12 5.00E·13 1.46E-14 4.00E-12 l.OOE-12 8/12/1991 2.77E-16 5.00E-12 1.25E-12 4.17E·17 8.00E-14 2.00E-14 1.45E-16 2.00E-12 S.OOE-13 1.80E·14 4.00E-12 l.OOE-12 11/11/1991 6.65E-17 5.00E-12 1.25E-12 9.13E·17 S.OOE-14 2.00E-14 2.77E-17 2.00E-12 5.00E-13 1.06E-14 4.00E-12 l.OOE-12 ,2/10/1992 1.94E-16 5.00E-12 1.25E-12 4.28E·17 S.OOE-14 2.00E-14 4.08E-17 2,00E-12 S.OOE-13 3.51E-14 4.00E-12 l.OOE-12 5/11/1992 2.54E-16 5.00E-12 1.25E-12 5.49E-16 S.OOE-14 2.00E-14 6.86E-17 2.00E-12 5.00E-13 1.38E-14 4.00E-12 l.OOE-12 8/10/1992 1.73E-16 5.00E-12 1.25E-12 1.55E·16 S.OOE-14 2.00E-14 1.20E-16 2.00E·12 S.OOE-13 1.53E-14 4.00E-12 l.OOE-12 11/9/1992 1.56E-16 5.00E-12 1.25E-12 3.19E·17 B.OOE-14 2.00E-14 4.90E-18 2.DOE·12 5,00E-13 1.86E-14 4.00E-12 l.OOE-12 2/9/1993 2.10E-16 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 3.89E-17 LOOE-12 5.00E-13 2.52E-14 4.00E-12 1.00E-12 5/10/1993 1.00E-16 S.OOE-12 1.25E-12 4.11E-17 S.OOE-14 2.00E-14 6.43E-17 2.00E·12 5.00E-13 1.26E-14 4.00E-12 l.OOE-12 8f10/1993 2.30E-16 S.OOE-12 1.25E-12 6.00E-17 S.OOE-14 2.00E-14 6.43E-17 2.00E·12 S.OOE-13 1.60E-14 4.00E-12 l.OOE-12 U/8/1993 S.OOE-12 1.25E-12 S.OOE-14 2.00E-14 O.OOE+OO 2,00E-12 S.OOE-13 L.57E-14 4.00E·12 1 OOE-12 2/7/1994 1.82E-16 S.OOE-12 1.25E-12 S,OOE-18 B.OOE-14 2.00E-14 4.30E-17 2.00E-12 S.OOE-13 2.59E-14 4.00E-12 1.00E-12 5/9/1994 3.60E·16 5.00E-12 1.25E·12 2.70E-16 S.OOE-14 2.00E-14 2.87E-16 2.00E-12 ~.OOE-13 1.60E-14 4.00E-12 l.OOE-12 8/9/1994 4.04E-16 5,00E-12 1.25E-12 2.70E-16 S.OOE-14 2.00E-14 2.94E-16 2.00E-12 5.00E·13 2.00E-15 4.00E-12 l.OOE-12 11/7/1994 9.18E-17 S,OOE-12 1.25E·12 3,60E-16 S.OOE-14 l .OOE-14 2.91E·16 Z.OOE-12 5.00E-13 2.00E-15 4.00E·12 l.OOE-12 --- Date 'Effluent Concentration Limit= 9E-14 uCi/ml BHV-1U Effluent Concentration Limit-2E-14 uCi/ml BHV-lT Effluent Concentration Limit-9E-13 uCi/ml BHV-1R Effluent Concentration Limit-6E-13 uCi/ml BHV-1PB ALARA Goal-2.25E-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal= Z.25E-13 uCi/ml ALARAGoal = l.SE-13 uCi/ml Pre 1994 MPC Limit= SE-12 uCijml Pre 1994 MPC Limit= SE-14 uCi/ml Pre.l994 MPC U(lllr:-2E-12 uCi/ml P~ 1994 MPC limlb 4E-12 uCi/ml Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC IFCA I Z/7/1995 1.77E-16 9.00E-14 2.25E-14 9.70E-17 2.00E-14 S.OOE-15 9.70E-17 9.00E-13 2.25E-13, 8.60E-15 6.00E-13 l.50E-13 5/9/1995 9.40E-17 9.00E-14 2.25E-14 5.36E-16 2.00E-14 S.OOE-15 1.60E-15 9.00E-13 2.25E-13 3.84E-15 6.00E-13 l.50E-13 I 8/9/1995 2.70E-16 9.00E-14 2.25E-14 1.60E-16 2.00E-14 S.OOE-15 2.76E-16 'J.OOE-13 2.25E-13 3.76E-15 6.00E-13 l.50E-13 11/11/1995 4.80E-15 9.00E-14 2.25E-14 6.41E-16 2.00E-14 S.OOE-15 8.93E-16 9.00E-13 2.25E-13 5.20E-15 6.00E-13 l.50E-13 I 2/5/1996 5.34E-15 9.00E-14 2.25E-14 2.30E-15 2.00E-14 S,OOE-15 1.30E-15 9.00E-13 2.25E-13 4.20E-15 6.00E-13 1.50E-13 I 5/6/1996 5.11E-16 9.00E-14 2.25E-14 3.06E-16 2.00E-14 S.OOE-15 1,40E-16 9.00E-13 2.25E-13 7.03E-15 6.00E-13 l.50E-13 8/5/1996 5.99E-16 9,00E-14 2.25E-14 1.55E-15 2.00E-14 S.OOE-15 2.03E-16 9.00E-13 2.25E-13 5.94E-15 6.00E-13 1.50E-13 11/6/1996 3.38E-16 9.00E-14 2.25E-14 ,5.45E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.22E-14 6.00E-13 l.50E-13 216/1997 l.OOE-16 9.00E-14 2.25E-14 1.25E-16 2.00E-14 S.OOE-15 1.28E-16 9.00E-13 2.25E-13 5.68E-15 6.00E-13 1.50E-13 5/5/1997 1.09E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 4.39E-15 6.00E-13 1,50E-13 8/11/1997 2.88E-16 9.00E-14 2.25E-14 3.83E-16 2.00E-14 S.OOE-15 1.82E-16 9,00E-13 2,25E-13 5,29E-15 6.00E-13 l.50E-13 1/5/1998 3.24E-16 9.00E-14 2.25E-14 3.47E-16 2.00E-14 S.OOE-15 1.19E-16 9.00E-13 2.25E-13 4.73E-15 6,00E-13 1.50E-13 4/28/1998 4.75E-16 9.00E-14 2.25E-14 6.73E-16 2.00E-14 S.OOE-15 5.69E-16 9.00E-13 2,25E-13 5.94E-15 ,G,OOE-13 l.50E-13 7/31/1998 8.84E-16 9.00E-14 2.25E-14 l.93E-15 2.00E-14 S,OOE-15 1.43E-15 9.00E-13 2.25E-13 5.22E-15 6,00E-13 1,50E-13 .9/28/1998 2.81E-16 9.00E-14 2.25E-14 2.89E-16 2.00E-14 5.00E-15 1.80E-16 9.00E-13 2.25E-13 4.64E-15 6.00E-13 l.50E-13 12/28/1998 8.08E-16 9.00E-14 2.25E-14 4.93E-16 2.00E-14 5.00E-15 5.01E-16 9.00E-13 2.25E-13 1.06E-14 6.00E-13 1.50E-13 3)2~/1999 2.06E-16 9.00E-14 2.25E-14 2.06E-16 2.00E-14 5,00E-15 1,42E-16 9.00E-13 2.25E-13 6.69E-15 6,00E-13 l.50E-13 7/3/1999 5.31E-16 9.00E-14 2.25E-14 .2.47E-16 2.00E-14 5.00E-15 2.23E-16 9.00E-13 2.25E·13 6.44E-15 6.00E-13 1.50E-13 9/27/1999 8.98E-16 9.00E-14 2.25E-14 .3.90E-16 2.00E-14 5,00E-15 2,96E-16 9.00E-13 2.25E-13 7,29E-15 6.00E-13 1.50E-13 12/28/1999 1.48E-15 9.00E-14 2.25E-14 6.00E-16 2.00E-14 5.00E-15 5.57E-16 9.00E-13 2.25E-13 6.19E-15 6.00E-13 1.50E-13 3/27/2000 l.OOE-16 9.00E-14 2.25E·14 l.06E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.23E-15 6.00E-13 1.50E-13 6}26!2000 3.47E-16 9.00E-14 2.25E·14 3.46E-16 2.00E-14 5.00E·15 3.62E-16 9.00E-13 2.25E-13 4.50E-15 6.00E-13 1.50E-13 9/26/2000 2.51E-16 9.00E-14 Z.25E-14 1.78E-16 2.00E-14 5.00E-15 3.25E-16 9,00E-13 2,25E-13 8.55E-15 6.00E-13 150E-13 12/26/2000 l.OOE-16 9.00E-14 2.25E-14 1.42E-16 .2.00E-14 5.00E-15 1.31E-16 9.00E-13 2.25E-13 7.77E-15 6.00E-13 1.50E-13 3/26/2001 3.10E-16 ~.OOE-14 2.25E-14 l.OOE-15 .2.00E-14 5.00E-15 l.OOE-15 9.00E-13 2.25E-13 7.19E-15 6.00E-13 1.50E-13 7/29/2001 1.52E-16 9.00E-14 2.25E-14 1.44E-16 2.00E-14 5.00E-15 1.77E-16 9.00E-13 2.25E-13 7.21E-15 6.00E-13 1.50E-13 9/24/2001 1.03E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.09E-15 6.00E-13 1.50E-13 12/31}2001 1,00E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.39E-15 6.00E-13 1.50E-13 4/1/2002 2.05E-16 9.00E-14 2.25E-14 2.44E-16 2.00E-14 5,00E-15 2.29E-16 9.00E-13 2.25E-13 8.15E-15 6.00E-13 1.50E-13 7/1/2002 3.55E-16 ~.OOE-14 2.25E-14 4.85E-16 2,00E-14 5,00E-15 1.06E-16 9.00E-13 2.25E-13 7.65E-15 6.00E-13 1.50E-13 9/30/2002 1.17E-16 9.00E-14 2.25E-14 1.61E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 3.68E-15 6.00E-13 1.50E-13 12/30/2002 l.OOE-16 9.00E-14 2.25E-14 1.03E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 9.46E-15 6.00E-13 1.50E-13 3}31/2003 1.20E-16 ~.OOE-14 2.25E-14 1.12E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 4.68E-15 6.00E-13 1.50E-13 6/30/2003 2.18E-16 9.00E-14 2.25E-14 MOE-16 2.00E-14 5.00E-15 1.67E-16 9.00E-13 2.25E-13 5.96E-15 6.00E-13 1.50E-13 9/29/2003 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.28E-15 6.00E-13 1.50E-13 12/29/2003 l.OOE-16 9,00E-14 2.25E-14 2.54E-16 2.00E-14 5,00E-15 3.35E-16 9.00E-13 2.25E-13 6.25E-15 6.00E-13 1,50E-13 3/29/2004 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.54E-14 6.00E-13 1.50E-13 6/27/2004 l.OOE-16 9.00E-14 .2.25E-14 l.OOE-16 .2.00E-14 5.00E-15 l,OOE-16 9.00E-13 2.25E-13 3.04E-15 6.00E-13 1.50E-13 9/27/2004 l.OOE-16 9,00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.05E-14 6.00E-13 1,50E-13 12/27/2004 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 LOOE-16 9.00E-13 2.25E-13 1.59E-14 6.00E-13 1.50E-13 3/28/2005 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 ~.OOE-13 2.25E-13 7.42E-15 6.00E-13 1.50E-13 6/29/2005 LOOE-16 9 OOE-14 2.25E-14 1.30E-16 2.00E-14 5.00E-15 1.20E-16 9.00E-13 2.25E-13 7.94E-15 6.00E-13 1.50E-13 9/26/2005 l.OOE-16 9.00E-14 2.25E-14 2,56E-16 2.00E-14 5.00E-15 2.42E-16 9.00E-13 2.25E-13 l.22E-14 6,00E-13 1.50E-13 1/3/2006 2.13E-16 9.00E-14 2.25E-14 1.04E-16 2 .. 00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 '3,73E-14 6.00E-13 1.50E-13 4/3/2006 1.62E-16 9.00E-14 2.25E-14 1.86E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.36E-15 6.00E-13 1.50E-13 7/3/2006 l.86E-16 9.00E-14 2,25E-14 l.OOE-16 ZcOOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 9.77E-15 6.00E-13 1.50E-13 10/2/2006 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 l.30E-14 6.00E-13 1.50E-13 1/1/2007 l.OOE-16 9.00E-14 2.25E-14 1.47E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.17E-14 6.00E-13 1.50E-13 4/2/2007 2.23E-16 9.00E-14 2.25E-14 1.63E-16 2.00E-14 5.00E-15 l.OOE-16 g.OOE-13 2.25E-13 1.65E-14 6.00E-13 1.50E-13 7/2/2007 3.35E-16 9.00E-14 2.25E-14 1.34E-16 2.00E-14 ,S.OOE-15 1.36E-16 9.00E-13 Z.25E-13 1.78E-14 6.00E-13 1.50E-13 9/30/2007 1.15E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 7.68E-15 6.00E-13 1.50E-13 12/31/2007 l.OOE-16 9,00E-14 2.25E-14 1.93E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 3/31/2008 1.14E-16 9,00E-14 2.25E-14 1.13E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 6.44E-15 6.00E-13 1.SOE-13 6/30/2008 7.09E-16 9,00E-14 2.25E-14 3.83E-16 2.,00E-14 S.OOE-15 2.27E-16 9.00E-13 I2.25E-13 6.52E-15 I6.00E-13 l.50E-13 Date ~ffluent Concentration Limit= 9E-14 uCi/ml BHV-1U Effluent Concentration Limit = ZE-14 uCijml BHV-lT Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = pE-13 uCi/ml BHV-1PB AlARAGoal = :Z.:ZSE-14 uCi/ml AlARA Goal= SE-13 uCi/ml AlARAGoal = 2.25E-13 uCi/ml AlARA Goal-l.SE-13 uCi/ml Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC Limit = SE-14 uCi/ml Pre 1994 MPC Limit = :ZE-12 uCi/ml Pte 1994 MI'C.Vmit-= 4E-12 uCi/ml Pre 1994 A lARA GOAL= 1.25E-12 uCi/ml Pre 1994 AlARA GOAL= SE-13 uCi/ml Pre 1994 AlARA GOAL = 1E-12 uCi/ml tone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC ~FCA 9/30/2008 7.69E-16 9.00E-14 2.25E-14 2.94E-16 2.00E-14 5.00E·15 1.90E-16 9.00E-13 2.25E-13 7.64E-15 6.00E-13 1.50E-13 12/31/2008 1.21E-15 9.00E-14 2.25E-14 4.76E-16 2.00E-14 5.00E·15 3.34E-16 9.00E·13 2.25E-13 1.16E-14 6.00E-13 1.50E-13 3/15/2009 2.14E-15 9.00E-14 2.25E-14 1.02E·15 2.00E·14 S.OOE-15 1,00E-15 9.00E-13 2.25E-13 4.44E-15 6.00E·13 1.50E-13 6}15/2009 5.97E-17 9.00E-14 2.25E-14 2.35E-16 .2,00E-14 5.00E-15 2.18E-16 9.00E-13 2 25E-13 5.13E-15 G.OOE-13 1.50E-13 9/15/2009 9.55E-16 9.00E-14 2.25E-14 1.71E-16 2.00E-14 5.00E-15 9.87E-17 9.00E-13 2.25E-13 9.47E-15 6.00E·13 1.50E-13 12/15/2009 1.24E-15 9.00E-14 2.25E-14 9.25E-17 2.00E-14 5,00E-15 5.60E-17 9.00E-13 2.25E-13 5.95E-15 G.OOE-13 1.50E-13 3/31/2010 1.97E-15 t.l.OOE-14 2.25E-14 2.15E-16 2.00E-14 5.00E-15 3.27E-16 9.00E-13 2.25E-13 1.00E-14 6.00E-13 1.50E-13 6/30/2010 1,58E-15 9.00E-14 2.25E-14 4.71E-16 Z.OOE-14 5.00E-15 7.70E-16 9.00E-13 2.25E-13 4.07E-15 6.00E-13 1.50E-13 9}30/2010 8.42E-16 9.00E-14 2.25E-14 2.80E-16 2.00E-14 5.00E-15 1.31E-16 9.00E-13 2.25E-13 6.80E-15 G.OOE-13 1,50E-13 12/31/2010 1.27E·15 9.00E-14 2.25E-14 2.32E-16 2.00E-14 5,00E-15 2.30E-16 9.00E-13 2.25E-13 1.27E-14 6.00E-13 1.50E-13 4/4/2011 9.01E-16 ll.OOE-14 2.25E-14 1.90E-16 2.00E-14 5,00E·15 3.64E-16 9.00E-13 2.25E-13 1,09E-14 6.00E-13 1.50E-13 7/4/2011 1.59E-15 9.00E-14 2.25E-14 5.31E-16 2.00E-14 5.00E-15 4.99E-16 9,00E-13 2.25E-13 8.38E-15 6.00E-13 1.50E-13 10/3/2011 2.92E-16 S.OOE-14 2.25E·14 1.17E-16 2.00E-14 5.00E-15 li76E-17 ~.OOE-13 2.25E-13 1.14E-14 6.00E-13 1,50E-13 1/3/2012 6.73E-16 9.00E-14 2.25E-14 1.19E-16 2.00E-14 S.OOE-15 8.58E-17 9.00E-13 2.25E-13 l .73E-14 G.OOE-13 l.SOE-13 4/3/2012 7.87E-16 9.00E-14 2.25E-14 2.64E-16 2.00E-14 ·s .OOE-15 3.95E-16 9.00E-13 2.25E-13 1.25E-14 G.OOE-13 1.50E-13 7/2/2012 1.86E-15 9,00E-14 2.25E-14 8.33E-16 2.00E-14 S.OOE-15 9.85E-16 9.00E-13 2.25E-13 9.55E-15 6.00E-13 1.50E-13 10/1/2012 1.06E-15 9.00E-14 2.25E-14 2.11E-16 2.00E-14 S.OOE-15 2.34E-16 9.00E-13 2.25E-13 1.13E-14 6.00E-13 1.50E-13 12/31/2012 6.86E-16 9.00E-14 2.25E-14 1.27E-16 2,00E-14 5.00E-15 1.38E-16 S.OOE-13 2.25E-13 1.54E-14 6.00E-13 1.50E-13 3/25/2013 9.91E-16 9.00E-14 2.25E-14 1.86E-16 2,00E-14 S.OOE-15 2.04E-16 9.00E-13 2.25E-13 1.82E-14 6.00E-13 1.50E-13 7/2/2013 1.46E-16 9.00E-14 2.25E-14 3.34E-16 2.00E-14 5.00E-15 3.91E-16 9.00E-13 2.25E-13 5.78E-15 6.00E-13 l.SOE-13 9/30/2013 8.89E-16 9.00E-14 2.25E-14 9.13E-17 2.00E-14 5.00E-15 1.05E-16 9.00E-13 2.25E-13 B.OOE-15 6.00E-13 1.50E-13 12/30/2013 5.21E-16 9,00E-14 2.25E-14 4.34E-17 2.00E-14 5.00E-15 3.70E-17 9.00E-13 2.25E-13 2,59E-14 6.00E-13 1.50E-13 3/31/2014 1.07E-15 9.00E-14 2.25E-14 2.07E-16 2.00E-14 S.OOE-15 3.69E-16 9.00E-13 2.25E-13 1.24E-14 6.00E-13 1.50E-13 6/30/2014 2.24E-15 9.00E-14 2.25E-14 6.14E-16 2.00E-14 S.OOE-15 1.09E-15 9.00E-13 2.25E-13 1.23E-14 p.OOE-13 1.50E-13 -.E 0 ::I -II) c: 0 ~ ... -c: Cl) (.) c: 0 0 Cl) "C (.) ::I c: 0 "C ca a: C\1 .- I w 0 ~ Ct) .- I w 0 0 .- .. ~ ~ J. • ~ ~ .. ;;;:_, !"-+- ~ ~ .. +::: ~ 411:; ~ ·=== ~ ""~ ,__ . .:; r- ...... ~ ~t.. 1:::... -, 1 41::;~ ....... _.;:. ,..~ ; "<!" .-I w 0 ~ ~ 8~-des .A ~ u-des I ~ ~ ""~ ~ I ~ ::. ~ • ~ 1-4 • ..... ~ .~ ~~-des o~-des 6o-des so-des I ~ I"'~ ~ ~ .. ~ Lo-des go-des go-des 0 .- C\1 ' va-des "0 ell Q) ~·-:. •• ~ 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I" ~ -~ -~t 1.4 ;1l i+= 1 .. o:::;;; ;;;.:~ ·=== ~ ~ ~::;;: -t--t. ~ •t_ IE .... •::::." .. :--- J ~-r-.. -• .;;;;P"' ~-....... r+- L{) .- I w 0 0 (are::>s oo1) I I" ~ ::s t y= ~ ~ .-'4 :::;:::... :;l ~ fi"' :::.t 4 .. 1-4 --. -. CD .- I w 0 ~ T""" ' ,..._ T""" I w 0 ~ T""" . - - - - - . co T""" I w 0 ~ 8~-das c~-das ~ ~-das o~-das 6o-das so-das La-das go-das so-das vo-das 8o-das co-das ~a-d as oo-das 66-das 95-das L6-das 95-das S6-das v6-das 86-das cm-das ~6-das 06-das 6s-das ss-das Ls-das gg-das ss-das vs-das 8s-das cs-das ~s-das -:§ 0 ::::J -tn c 0 i ... -c Q) u c 0 0 co C\1 C\1 I E ::::J "C co a: ,.... :> ::I: m ,.,-.... ,.... C\1 ,.... ,.... w I w 0 0 ~ ~ ,.... ,.... .... .. 4 -=: ~ 4<:: I .. .-~~ ~ ('I) "¢ l.() ,.... ,.... ,.... I I I w w w 0 0 0 ~ 0 0 'iaiBOS 6o1f ~ ~ ~~ r. ~1 "'-' ~ f--' ~~ h ~ • ~ ·-== ~ • k! -~ t::: P--~ :::. :, .~ • r ,.;-- ~ ... I ~ { le """' • ~. :::. .. _It :-4 co ,.... I w 0 ~ • I'-,.... I w 0 ~ - . ' ex:> ,.... I w 0 ~ 8~-das c~-das ~~-des o~-das 6o-das so-das La-das go-des so-das vo-das 8o-das co-das ~o-des oo-das 66-das 86-das L6-das 95-das 95-das 175-das 86-das c6-das ~5-das 06-das 6e-das ee-das Le-das gg-das gg-das ve-das 88-das ce-des ~e-das - 0 c: 0 ;; C'CI ... -c: Cl) (,) c: 0 (.) 0 'f"'" ~ "C C'CI Cl) ..J 'f"'" > ::I: m ..... I UJ 0 C! C\J ('I) ..... ..... I I UJ UJ 0 0 C! C! ..... ,.., ~I ~~ I~ J. ~ •I • ~ ~ ... ;;;:;;. --... ~ • =-~ • ~ ~ ~ • • ;It~ ~ i « ~ I.C:::: ~ ~ ....... -«:; ........ .._ I •-.:: ~ ~l. :::.. -, 16. Ill=:::; t 1•:::::: ~ _.;~ ""I== J "'d" uJ 0 0 (are~s Bo1) ~ 1.0 c.o ..... ..... I I UJ UJ 0 0 C! C! ,... . . . . - . " . 1"-..... I UJ 0 C! 8~-das c~-das ~ ~-das o~-das 6o-das so-das La-das go-d as so-das vo-das so-das co-das w -das oo-das 66-das 95-das L6-das 96-das 95-das v6-das 86-das c6-das ~6-das 06-das 6s-das ss-das La-das gs-das ss-das vs-das ss-das cs-das ~s-das TAB2 BHV-2 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-ZU :effluent Concentration Limit= ZE-14 uCi/ml BHV-ZT Effluent Concentration Limit-9E-13 uCi/ml BHV-ZR ~ffluent Concentration Limit= 6E-13 uCi/ml BHV-ZPB ALARAGoal-Z.ZSE-14 uCi/ml ALARA Goal-SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARAGoal-1.SE·13 uCi/ml_ Pre..l994 MPC Lil'l11t = , SE-12 uCi/ml Pre 1994 MPC Limit= SE-14 uCi/ml Pre J.li9,4 MpCUmlt"-2E-12 uC[/ml .Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 A LARA GOAL= 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA tone EFC EFCA Cone EFC EFCA 9/28/1981 1.39£-15 S.OOE-12 1.25£-12 3.69£-16 8.00£-14 2.00£-14 5.92£-16 Z.OOE-12 S.OOE-13 l.67E-14 4.00£-12 l.OOE-12 12/14/1981 4.62£-16 S.OOE-12 1.25£-12 8.03£-16 8.00£-14 2.00E-14 3.62£-16 2.00£-12 S.OOE-13 133E-14 4.00£-12 l.OOE-12 3/29/1982 7.07£-16 S.OOE-12 1.25E-12 l.lOE-15 8.00£-14 2.00E-14 '7.27E-16 2.00E-12 p.OOE-13 1.52£-14 4.00E-12 l.OOE-12 6/30/1982 8.84£-16 5.00£-12 1.25£-12 7.73£-16 8.00£-14 2.00E-14 4.78£-16 2.00£-12 S.OOE-13 1.98£-14 4.00£-12 l.OOE-12 9/27/1982 1.23£-15 5.00£-12 1.25E-12 3.60£-16 8.00£-14 2.00E-14 8.73£-16 2.00E-12 S.OOE-13 2,35£-14 4.00E-12 1,00£-12 1/3/1983 2.64E-15 S.OOE-12 1.25E-12 2.S5E-16 8.00£-14 2.00£-14 1.98£-16 Z.OOE-12 l>.OOE-13 2.85£-14 4.00E-12 l.OOE-12 4/4/1983 2.14E-16 S.OOE-12 1.25E-12 1.02£-16 8,00£-14 2.00£-14 1.57£-16 2.00E-12 S.OOE-13 2.48£-14 4.00£-12 l.OOE-12 6/30/1983 2.85£-16 5.00£-12 1.25E-12 2.06£-16 8.00E-14 2.00E-14 ,2.24£-16 Z.OOE-12 S.OOE-13 1.79£-14 4.00£-12 1.00E-12 10/3/1983 .2.70£-16 5.00£-12 1.25E-12 3.36£-16 8.00£-14 2.00E-14 4.37£-16 :Z.OOE-12 ~.OOE-13 1.78£-14 4.00£-12 1.00£-12 1/3/1984 .2.78£-15 5.00£-12 1.25E-12 1.20£-16 8,00£-14 2.00E-14 'p.64E-17 2.00£-12 S.OOE-13 9.14E-15 4,00E-12 1.00E-12 4/2/1984 4.28E-16 5.00£-12 1.25E-12 1.75E-16 8.00£-14 2.00E-14 4.57E-17 2,00£-12 ,S.OOE-13 3.55£-14 4.00E-12 1.00£-12 7/2/1984 .2.78E-15 S.OOE-12 1.25£-12 8.12£-16 8,00£-14 2.00£-14 1.98E-16 2.00£-12 S.OOE-13 1.68£-14 4.00£-12 1.00E-12 10/1/1984 2,69E-16 '5.00£-12 1.25E-12 2.66E-17 8.00£-14 2.00E-14 O.OOE+OO 2.00£-12 S.OOE-13 1.77£-14 4.00£-12 1.00£-12 1/2/1985 2.15E-16 '5.00£-12 1.25E-12 7.55£-16 8.00£-14 2.00E-14 .2.87£-16 Z.OOE-12 S.OOE-13 H9E-14 4.00£-12 1.00E-12 4/1/1985 l.OOE-16 5.00£-12 1.25E-12 1.67£-16 8.00£-14 2.00E-14 6.75£-17 Z.OOE-12 S.OOE-13 7.56£-15 4.00£-12 1.00E-12 7/1/1985 .3.70£-17 5.00£-12 1.25E-12 9.00£-16 8.00£-14 2.00£-14 4.90£-17 2.00£-12 /).OOE-13 1.31£-14 4.00£-12 l.OOE-12 9/30/1985 9.32£-17 S.OOE-12 1.25E·12 2.18£-16 8.00£-14 2.00E-14 3.71£-16 2.00E·12 S.OOE-13 3.64£-15 4.00E-12 l.OOE-12 1]2/1986 l.OOE-16 S.OOE-12 1.25E-12 2.16E-16 8.00E-14 2.00E-14 :Z.15E·17 2.00E-12 5.00E·13 ,3,04E·16 4.00E·12 1,00£-12 4]1/1986 1.31£-15 5.00£-12 1.25£-12 1.SOE-16 8.00£-14 2.00E-14 3.71£-16 2.00E·12 5.00£-13 2.90£-15 4.00E-12 l.OOE-12 6/30/1986 2.23£-16 5.00£-12 1.25E-12 1.32£-16 8.00E-14 2.00E-14 '7.09£-17 2.00£-12 5.00E-13 2.53E·14 4.00E·12 l.OOE-12 10/27/1986 15.41E-16 S.OOE-12 1.25E-12 1.74£-16 8.00E-14 2.00E-14 3.67£-16 2.00E-12 5.00E·13 1.04£-14 4.00E·12 l.OOE-12 12/15/1986 3.56E-16 $.00£-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 1.05£-16 2.00£-12 5.00E-13 7.81E·15 4.00E·12 l.OOE-12 3/16/1987 5.31£-16 5.00£-12 1.25E·12 1.30E-16 8.00E-14 2.00E-14 7.74£-17 2.00£-12 5.00E·13 8.80£-14 4.00E·12 l.OOE-12 5/11/1987 4.06£-16 S.OOE-12 1.25E·12 6.63£-17 8.00£-14 2.00£-14 1.34£-16 2.00E·12 S.OOE-13 l.lOE-14 4.00£-12 l.OOE-12 9/9/1987 2.74£-16 S.OOE-12 1.25E·12 2.38E-16 8.00E-14 2.00E·14 1.38£-16 2.00E-12 5.00E·13 1.04£-14 4.00£-12 1,00£-12 11/2/1987 3.73£-16 S.OOE-12 1.25E·12 3.11E·16 8.00E·14 2.00E·14 L83E-16 2.00E·12 5.00£-13 L17E-14 4.00£-12 l.OOE-12 2/16/1988 2.78£-15 S.OOE-12 1.25E-12 2.31E-17 8.00E-14 2.00E-14 1.20£-16 2.00E-12 5.00E·13 3.55E·14 4.00E·12 l.OOE-12 5/18/1988 4.63E-16 5.00£-12 1.25E·12 1.49E-16 B.OOE-14 2.00E·14 2.30£-16 2.00E-12 5.00E·13 1.18£-14 4.00£-12 l.OOE-12 8/15/1988 8.06E·16 S.OOE-12 1.25E-12 8.69£-16 B.OOE-14 2,00E-14 1.80£-16 2.00E·12 5.00E-13 1.42E-14 4.00E-12 l.OOE-12 11/14/1988 4.34£-16 S.OOE-12 1.25E·12 6.76E·16 8.00E·14 2.00E-14 1.57£-16 2.00E-12 5.00£-13 11.25£-14 4.00E-12 l.OOE-12 2/13/1989 5.80£-16 S.OOE-12 1.25E-12 2.85£-16 8.00E-14 2.00£-14 1.55£-16 2.00E-12 5.00E-13 2.80£-14 4.00E-12 l.OOE-12 5/15/1989 5.06£-16 S.OOE-12 1.25£-12 2.28£-16 8.00E-14 2.00£-14 1.63E-16 2.00E-12 5.00E-13 6.05£-15 4.00E-12 l.OOE-12 8/14/1989 4.71£-16 5,00£-12 1.25E-12 9.60E-16 8.00E-14 2.00E-14 1.26E-15 2.00E-12 5.00E-13 6.65E-15 4.00E-12 l.OOE-12 11/13/1989 1.14£-15 S.OOE-12 1.25E-12 4.08E-16 8.00E-14 2.00£-14 4.18£-16 2.00E-12 5.00£-13 1.59E-14 4.00E-12 l.OOE-12 2}12/1990 1.09£-15 ,S.OOE-12 1.25E-12 3.25E-16 8.00E-14 2.00£-14 3.74£-16 2.00E-12 5.00£-13 1.98E-14 4.00£-12 l.OOE-12 5/14/1990 9.32£-16 5.00£-12 1.25E-12 5.27£-16 8.00£-14 2.00£-14 3.97£-16 2.00E-12 5.00£-13 1.69E-14 4.00£-12 l.OOE-12 8/13/1990 1.66£-16 5.00£-12 1.25£-12 5.49£-16 8.00£-14 2.00E-14 4.75£-17 2.00E-12 5.00E-13 1.27E-15 4.00E-12 l.OOE-12 11/12/1990 6.05£-16 S.OOE-12 1.25E-12 2.64E-16 8.00E-14 2.00£-14 1.93E-16 2.00E-12 5.00E-13 2.25E-14 4.00£-12 l.OOE-12 2/11]1991 8.72£-17 5.00£-12 1.25£-12 ?.OOE-18 8.00E-14 2.00£-14 3.33E-17 2.00£-12 5.00E-13 3.49£-14 4.00E-12 l.OOE-12 5/13/1991 1.16£-16 S.OOE-12 1.25E-12 3.86E-16 8.00E-14 2.00£-14 2.80E-16 2.00E-12 5.00E-13 1.50E-14 4,00£-12 l.OOE-12 8/12/1991 9.02E-17 p.OOE-12 1.25£-12 8.82E-17 8.00E-14 2.00£-14 7.65£-17 2.00E-12 5.00E-13 1.58E-14 4.00E-12 l.OOE-12 11/11/1991 4.81£-17 5.00£-12 1.25£-12 3.82E-17 8.00E-14 2.00£-14 2.54£-17 2.00E-12 5.00£-13 1.45E-14 4.00£-12 l.OOE-12 2/10/1992 1.54£-16 5.00£-12 1.25£-12 p.82E-17 8.00E-14 2,00£-14 1.40E-17 2.00E-12 5.00£-13 3.41E-14 4.00£-12 1.00E-12 5/11/1992 2.38£-16 5.00E-12 1.25£-12 7.63E-17 S.OOE-14 2,00£-14 3.07E-17 2.00E-12 5.00£-13 1.27E-14 4,00E-12 l.OOE-12 8/10/1992 1.01£-16 S.OOE-12 1.25£-12 7.07E-17 8.00E-14 2 OOE-14 2.80E-17 2.00E-12 5.00£-13 1.41£-14 4.00£-12 l.OOE-12 11/9/1992 5.20£-17 5.00£-12 1.25£-12 3.65E-17 8.00E-14 Z.OOE-14 1.78E-17 2.00E-12 5.00E-13 1.71E-14 4.00E-12 l.OOE-12 2/9/1993 2.39£-16 S.OOE-12 1.25£-12 2.97E-17 8.00E-14 2,00£-14 6.31E-17 2.00£-12 5.00E-13 3.41E-14 4.00E-12 l.OOE-12 5/10/1993 l.OOE-16 S.OOE-12 1.25E-12 7.11E-17 8.00E-14 2.00E-14 3.19E-17 2.00E-12 5.00E-13 1.34E-14 4.00E-12 l.OOE-12 8/10/1993 1.90E-16 S.OOE-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 5.00E-13 1.80E-14 4.00E-12 l.OOE-12 11/8/1993 l.OOE-16 S.OOE-12 1.25E-12 l.OOE-16 8.00£-14 2.00£-14 l.OOE-16 2.00E-12 5.00E-13 1.49E-14 4,00E-12 l.OOE-12 2/7/1994 2.23E-16 5.00£-12 1.25E-12 l.OOE-16 8.00£-14 2.00E-14 1.84£-16 2.00E-12 5.00£-13 2.19£-14 4.00£-12 l.OOE-12 5/9/1994 2.16E-16 5.00E-12 1.25E-12 7.20E-17 8.00E-14 2.00E-14 9.89£-17 2.00E-12 5.00E-13 1.37£-14 4.00£-12 l.OOE-12 8/9/1994 9.29£-17 S.OOE-12 1.25E-12 2.96E-16 8.00E-14 2.00E-14 3.04£-16 2.00E-12 5.00E-13 l.OOE-16 4.00E-12 l.OOE-12 11/7/1994 9.21E-17 S.OOE-12 1.25E-12 2.35E-16 8.00E-14 2.00E-14 1,00£-16 2.00E-12 5.00E-13 l.OOE-16 4.00E-12 1 OOE-12 - bate Effluent Concentration Limit= 9E-14 uCi/ml BHV-ZU Effluent Concentration Limit= 2E-14 uCi/ml BHV-2T Effluent Concentration Limit = 9E-13 uCi/ml BHV-2R Effluent Concentration Limit= 6E-13 uCi/ml BHV-2PB ALARA Goal= 2.25E-14 uCi/ml ALARAGoal = .SE-13 uCi/ml ALARA Goal= 2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC Limit = BE-14 uCi/ml Pre 1994 MPC Limit-2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 A LARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 1.18E-16 9.00E-14 2.25E-14 9.70E-17 .l.OOE-14 5.00E-15 9.70E-17 9.00E-13 2.25E-13 7.42E-15 6.00E-13 1.50E-13 S/9/1995 9.40E-17 9.00E-14 2.25E-14 1.20E-16 2.00E-14 5.00E-15 3.50E-16 9.00E-13 2.25E-13 3.90E-15 6.00E-13 1.50E-13 '8/9/1995 8.90E-17 9.00E-14 2.25E-14 9.67E-17 l .OOE-14 5.00E-15 1.35E-16 9.00E-13 2.25E-13 2.38E-16 6.00E-13 1.50E-13 11/11/1995 2.83E-15 9.00E-14 2.25E-14 4.09E-16 2.00E-14 5.00E-15 5.23E-16 9.00E-13 2.25E-13 6.77E-15 6.00E-13 1.50E-13 .2/5/1996 1.75E-15 9.00E-14 2.25E-14 8.66E-16 .2.00E-14 5.00E-15, 4.86E-16 9.00E-13 2.25E-13 3.50E-15 6.00E-13 1.50E-13 5/6}1996 1.40E-16 9.00E-14 ~.25E-14 1.15E-16 2.00E-14 '>.OOE-15 l.OOE-16 9.00E-13 2.25E-13 6.85E-15 6.00E-13 1.50E-13 8/5}1996 1.43E-16 9.00E-14 ;1.25E-14 2.78E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 ,5.83E-15 6.00E-13 1.50E-13 11/6/1996 1.45E-16 9.00E-14 2.25E-14 1.57E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.19E-14 6.00E-13 1.50E-13 2/6/1997 1.00E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.84E-16 6.00E-13 1.50E-13 5/5/1997 l.OOE-16 9.00E-14 .2.25E-14 l.OOE-16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 3.89E-15 6.00E-13 1.50E-13 8/11/1997 l.OOE-16 9.00E-14 2.25E-14 1.09E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.69E-15 6.00E-13 1.50E-13 1/5/1998 2.55E-16 9.00E-14 ,2.25E-14 1.07E-16 ,2.00E-14 5.00E-15 5.00E-17 9.00E-13 2.25E-13 5.11E-15 6.00E-13 1.50E-13 4/28/1998 1.20E-16 9.00E-14 2.25E-14 1.71E-16 2.00E-14 5.00E-15 1.28E-16 9.00E-13 2.25E-13 6.40E-15 6.00E-13 1.50E-13 7/31/1998 1.47E-16 9.00E-14 2,25E-14 4.24E-16 2.00E-14 5.00E-15 3.39E-16 9.00E-13 2.25E-13 4.80E-15 6.00E-13 1.50E-13 9/28/1998 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 l.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 4.26E-15 6.00E-13 1.50E-13 12/28/1998 2.54E-16 9.00E-14 2.25E-14 2.15E-16 2.00E-14 5.00E-15 1.38E-16 9.00E-13 2.25E-13 6.88E-15 6.00E-13 1.50E-13 3/29/1999 1.07E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.61E-15 6.00E-13 1.50E-13 7/3/1999 2.46E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.95E-15 6.00E-13 1.50E-13 '9/27/1999 2.81E-16 9.00E-14 2.25E-14 1.41E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2,25E-13 7.35E-15 6.00E-13 1.50E-13 12/28/1999 5.20E-16 9.00E-14 2.25.E-14 2.60E-16 2.00E-14 5,00E-15 2.01E-16 9.00E-13 2.25E-13 7.00E-15 6.00E-13 1.50E-13 3/27/2000 l.OOE-16 9.00E-14 2,25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.12E-15 6.00E-13 1.50E-13 6/26/2000 l.lOE-16 9.00E-14 2.25E-14 l.OOE-16 l.OOE-14 5.00E-15 1.16E-16 9.00E-13 2.25E-13 5.07E-15 6.00E-13 1.50E-13 'l/26/2000 l.OOE-16 9.00E-14 .2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.31E-15 6,00E-13 1.50E-13 12/26/2000 1.26E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 9.45E-15 6,00E-13 1.50E-13 3/26/2001 l.OOE-16 9.00E-14 ,2.25E-14 l.OOE-16 ,2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.95E-15 6,00E-13 1.50E-13 7/2/2001 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 l.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.56E-15 6.00E-13 1.50E-13 9/24/2001 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9 OOE-13 2 25E-13 6.16E-15 6.00E-13 1.50E-13 12/31/2001 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 2.20E-15 6.00E-13 1.50E-13 4/1/2002 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 9.95E-15 6.00E-13 1.50E-13 7/1/2002 1.25E-16 9.00E-14 2.25E-14 1.43E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.25E-15 6.00E-13 1.50E-13 9/30/2002 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 3.69E-15 6.00E-13 1.50E-13 12/30/2002 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 .l.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.91E-15 6.00E-13 1.50E-13 3/31/2003 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.16E-15 6.00E-13 1.50E-13 6/30/2003 l.OOE-16 9.00E-14 .2.25E-14 l.OOE-16 .l.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.27E-15 6.00E-13 1.50E-13 9/29/2003 l.OOE-16 9.00E-14 2,25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.23E-15 6.00E-13 1.50E-13 12/29/2003 l.OOE-16 9.00E-14 ,2.25E-14 l.OOE-16 ,2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.80E-15 6.00E-13 1.50E-13 3/29/2004 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 2.04E-14 6.00E-13 1.50E-13 6/27/2004 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9 OOE-13 2.25E-13 3.09E-15 6.00E-13 1.50E-13 9/27/2004 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 1.73E-14 6.00E-13 1.50E-13 12/27/2004 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2,25E-13 1.30E-14 6.00E-13 1.50E-13 3/28/2005 l.OOE-16 9.00E-14 2,25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9,00E-13 2.25E-13 8.88E-15 6,00E-13 1.50E-13 6/29/2005 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9,00E-13 2,25E-13 8.85E-15 6.00E-13 1.50E-13 9/26/2005 l.OOE-16 9.00E-14 ,2.25E-14 1.99E-16 .l.OOE-14 5.00E-15 1.44E-16 9,00E-13 2,25E-13 3.81E-14 6,00E-13 1,50E-13 1/3/2006 1.29E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 4.08E-16 9.00E-13 2.25E-13 6.58E-14 6.00E-13 1,50E-13 4/3/2006 1.02E-16 9.00E-14 ,2.25E-14 l.OOE-16 ,2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.08E-14 6,00E-13 1.50E-13 7/3/2006 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 l.lOE-14 6.00E-13 1.50E-13 10/2/2006 1.30E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.68E-14 6,00E-13 1.50E-13 1/1/2007 1.24E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 1.38E-14 6.00E-13 1.50E-13 4/2/2007 1.40E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.63E-14 6.00E-13 1.50E-13 7/2/2007 1.04E-16 9.00E-14 2.25E-14 l.OOE-16 7-00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.36E-14 6.00E-13 1.50E-13 9/30/2007 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 l.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.24E-15 6.00E-13 1.50E-13 12/31/2007 1.91E-16 9.00E-14 ,2.25E-14 l.OOE-16 ,2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.18E-14 6.00E-13 1.50E-13 3/30/2008 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.49E-15 6.00E-13 1.50E-13 6/30/2008 1.29E-16 9.00E-14 :2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1,00E-16 9.00E-13 2.25E-13 4.82E-15 6.00E-13 1.50E-13 Date Effluent Concentration Limit = 9E-14 u(i/ml BHV-2U Effluent Concentration Limit -ZE-14 uCi/ml BHV-2T Effluent Concentration Limit-9E-13 uCi}ml BHV-2R Effluent Concentration Limit= 6E-13 uCi/ml BHV-2PB ALARAGoal = 2.25E-14 uCi/ml ALARA Goal-SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml Pre 1994 MPC Limit-SE-12 uCi/ml Pre 1994 MPC"timlt= BE-14 uCi/ml , Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL= l.25E-12 uC[/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL= 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/3Q/2008 2.73E-16 9.00E-14 2.25E-14 1.00E-16 2,00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 8.30E-15 6.00E-13 1.50E-13 12/31/2008 5,71E-16 9.00E-14 Z.25E-14 1.61E-16 2.00E-14 5.00E-15 1.25E-16 9.00E-13 2.25E-13 2.04E-14 6.00E-13 1.50E-13 3/15/2009 3.96E-16 9.00E-14 2.25E-14 1.38E-16 2.00E-14 5.00E-15 1.07E-16 9.00E-13 2 25E-13 4.81E-15 6.00E-13 1.50E-13 6/15/2009 1.24E-17 9.00E-14 2.25E-14 4.64E-17 2.00E-14 5.00E-15 5.11E-17 9.00E-13 2.25E-13 4.58E-15 6.00E-13 1.50E-13 9/15/2009 2.43E-16 9.00E-14 2.25E-14 5.28E-17 2.00E-14 5.00E-15 4.84E-17 9.00E-13 2.25E-13 1.19E-14 6.00E-13 1.50E-13 12/15/2009 5.72E-16 9.00E-14 2.25E-14 2.94E-17 Z.OOE-14 5,00E-15 2.57E-17 9.00E-13 2.25E-13 6.70E-15 6.00E-13 1.50E-13 3/31/2010 5.47E-16 9.00E-14 2.25E-14 1.42E-17 2.00E-14 5,00E-15 4.66E-17 9.00E-13 2.25E-13 8.24E-15 6.00E-13 1.50E-13 6/30/2010 3.58E-16 9.00E-14 2.25E-14 6.64E-17 2.00E-14 5.00E-15 9.90E-17 9.00E-13 2.25E-13 .2.01E-15 6.00E-13 l.50E-13 9/30/2010 2.91E-16 9.00E-14 2.25E-14 4.48E-17 Z.OOE-14 5.00E-15 S.72E-17 9.00E-13 2.25E-13 l.OBE-15 6.00E-13 1.50E-13 12/31/2010 5.73E-16 .9.00E-14 2.25E-14 7.24E-17 2.00E-14 5.00E-15 .6.76E-17 9.00E-13 2.25E-13 1.35E-14 6.00E-13 1.50E-13 4/4/2011 3.79E-16 9.00E-14 2.25E-14 4.01E-17 2.00E-14 5.00E-15 9.11E-17 9,00E-13 .2.25E-13 1.06E-14 6.00E-13 1.50E-13 7/4/2011 3.07E-16 9.00E-14 2.25E-14 8.54E-17 2,00E-14 5.00E-15 9.21E-17 9.00E-13 2.25E-13 7.21E-15 G.OOE-13 1.50E-13 10/3/2011 1.17E-16 9.00E-14 2.25E-14 3,04E-17 2,00E-14 5.00E-15 .2.81E-17 9.00E-13 2.25E-13 1.03E-14 6.00E-13 1.50E-13 1/3/2012 ,3,65E-16 9.00E-14 2.25E-14 2.72E-17 2.00E-14 5.00E-15 4.54E-17 9.00E-13 2.25E-13 1.58E-14 G.OOE-13 1.50E-13 4/3/2012 4.22E-16 9.00E-14 2.25E-14 1.15E-16 Z.OOE-14 5.00E-15 ;2.77E-16 9.00E-13 2.25E-13 1.58E-14 p.OOE-13 1.50E-13 7/2/2012 3.39E-16 9.00E-14 2.25E-14 1.56E-16 2.00E-14 5.00E-15 1.74E-16 9.00E-13 2.25E-13 8.60E-15 6.00E-13 1.50E-13 10/1/2012 3.13E-16 9.00E-14 2.25E-14 4.13E-17 Z.OOE-14 5.00E-15 3.04E-17 9.00E-13 2.25E-13 1.03E-14 6.00E-13 1.50E-13 12/31/2012 1.76E-16 9.00E-14 2.25E-14 5.41E-17 Z.OOE-14 5.00E-15 7.05E-17 9.00E-13 .2.25E-13 1.48E-14 6.00E-13 1.50E-13 3/25/2013 .3.38E-16 9.00E-14 2 25E-14 3.94E-17 2.00E-14 5.00E-15 8.32E-17 9.00E-13 2.25E-13 1.42E-14 6.00E-13 1.50E-13 7/2/2013 4.06E-16 9.00E-14 2.25E-14 4.89E-17 Z.OOE-14 5.00E-15 8.06E-17 9.00E-13 2.25E-13 4.93E-15 6.00E-13 1.50E-13 9/30/2013 1.76E-16 9.00E-14 2.15E-14 2.52E-17 2.00E-14 5.00E-15 6.13E-17 9.00E-13 2.25E-13 4.90E-15 6.00E-13 1.50E-13 12/30/2013 6.20E-16 9.00E-14 2.25E-14 4.19E-17 2.00E-14 5.00E-15 3.72E-17 9.00E-13 2.25E-13 r5oE-14 6.00E-13 1.50E-13 3}31/2014 4.63E-16 9.00E-14 2.25E-14 4.97E-17 2.00E-14 5.00E-15 1.15E-16 9.00E-13 2.25E-13 1.49E-14 S.OOE-13 1.50E-13 6/30/2014 3.04E-16 9.00E-14 2.25E-14 7.92E-17 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 1.21E-14 p.OOE-13 1.50E-13 -E ~ 0 ::::J -en c 0 ~ -c G) (,) c 0 0 G) "C (,) ::::J c .52 "C C'CS a: N > J: m N w 0 ~ ..- I• r-.-... 4 I+ f::: I• F I• ~ ~ I• "== ... .. ~ .~ ~ Ct) ..- I LlJ 0 ~ ~ :2 ~ • ...:::; ~ L_ ..... ~ ~ l c 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(\j (I') ,...-,...- I I UJ UJ 0 0 ~ ~ ,...-,...- 1..::: .... r- ,. ...... --=: ~ .... 4 If' I=: ..- ~~ .r '<:t 1.() ,...-,...- I I UJ UJ 0 0 0 ~ (a1e::>s Eiol) ....... ~ 41 -r..... < ~ -... ~ ~ Ki ~ ~ ~ co ,...- I UJ 0 ~ ,...- ~ ~· ~~ ~ ~ :.4 ~t: .... ~ ~ - - - - - . - - ['-. ,...- I UJ 0 ~ 8 ~-das c~-das ~ ~-das o~-das 6o-das so-das La-das go-das so-das vo-das 8o-das co-das w -das oo-das 66-das 95-das L6-das 95-das 95-das 175-das 86-das c6-das ~6-das 06-das 6a-das aa-das La-das ga-das sa-das va-das 8a-das ca-das ~a-das U) c 0 +=i C'a """ -c Cl.) (.) c 0 () 0 ..... N I "C C'a Cl.) ..J N > ::I: Ill ..-. LU 0 0 I C\J C') ..-..-. . LU LU 0 0 ~ ~ ..-..- ec ~ ~ J. ~ ~ • I ~ ~ ~ .. ..._ r-.. ~ . .,.:::: ~ ~· • 4 , ~ !II + ~ • ~ ~ ~ ~ 1•=::: ~ ~,..,. t- ..:; ~ .... t:!>. ~t... ~ I' ro:::::: t .=::::: N ~F: .,..j. ;~ ~ ..-. LU 0 0 (aiBOS DOl) ~ LO <D ..-..-. . LU LU 0 0 ~ ~ ..- . - - . 1'--..-. LU 0 ~ 8~-das ~~-das ~ ~-das o~-das 6o-das so-das Lo-das go-das go-das vo-das 8o-das ~o-das ~o-das oo-das 66-das 86-das L6-das 96-das 96-das v6-das 86-das ~6-das ~6-das 06-das 6e-das se-d as La-das gg-das gg-das ve-das 8e-das ~e-das ~e-das TAB3 BHV-3 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit= 9E-14 uCi/ml .BHV-3U Effluent Concentration Limit = ZE-14 uCi/ml BHV-3T Effluent Concentration Limit= 9E-13 uCi/ml aHV-3R Effluent Concentration Limit= 6E-13 uCi/ml BHV-3PB AlARAGoal-2.Z5E·14 uCi/ml AlARAGoal-SE-13 uCi/ml ALARAGoal = 2.Z5E-13 uCi/ml AlARAGoal= 1.5E-13 uCi/ml Prn-1994 MPC Limit~ SE-12 uCi/ml Pre 1994 MPC Limit = SE-14 uCi/ml Pre 1994 MPC Umlr-< 2E-1Z uCi/ml Pre 1994 MPC Limit = IIE-12 uCi/ml Pre 1994 AlARA GOAL= l.ZSE-12 uCi/ml Pre 1994 ALARA GOAL= 5E·13 uCi/ml Pre 1994 AlARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 1.74E-15 S.OOE-12 1.25E-12 9.02E-16 8.00E-14 2.00E-14 2.87E-16 2.00E·12 S.OOE-13 1.54E-14 4.00E-12 1.00E-12 12/14/1981 1.59E-15 S.OOE-12 1.25E-12 5.03E-16 8.00E-14 2.00E-14 1.30E-16 2.00E-12 S.OOE-13 2.2SE-14 4.00E·l 2 l.OOE-12 3/29/1982 3.76E-16 S.OOE-12 1.25£-12 5.25£-16 8.00£-14 2.00£-14 4.08£-16 2.00£-12 S.OOE-13 1.96£-14 4.00£-12 l.OOE-12 6/30/1982 3.83E-16 5,00£-12 1.25£-12 2.16£-16 8.00£-14 2.00£-14 1.41£-15 2.00£-12 5.00£-13 2.40£-14 4.00£-12 l.OOE-12 9/27/1982 5.95E-16 5.00E-12 1.25E-12 1.44£-15 8.00£-14 2.00£-14 5.36£-16 2 OOE-12 S.OOE-13 1.43£-14 4.00£-12 l.OOE-12 1/3/1983 2.05E-16 S.OOE-12 1.25£-12 1.23E-16 8.00E-14 2.00£-14 l.lOE-16 2.00£-12 S.OOE-13 3.01E-14 4.00£-12 1.00E-12 4/4/1983 l.OOE-16 5.00E-12 1.25E-12 6.94E-17 8.00E-14 2.00£-14 6.11£-17 2.00E-12 S.OOE-13 1.39E-14 4.00£-12 l.OOE-12 6/30/1983 3.06E-16 5.00E-12 1.25E-12 9.59E-17 8.00E-14 2.00E-14 2.08E-16 2.00E-12 5.00E-13 1.70E-14 4.00E-12 l.OOE-12 10/3/1983 1.91E-16 5.00E-12 1.25£-12 3.05E-16 8.00£-14 2.00E-14 2.79£-16 2.00£-12 5.00£-13 1.76£-14 4.00£-12 l.OOE-12 1/3/1984 3,01£-16 5.00E-12 1.25£-12 9.51E-17 8.00£-14 2.00£-14 1,00£-16 2,00E·12 5.00E-13 9.17£-15 4.00£-12 l.OOE-12 4/2/1984 8.22£-16 5.00£-12 1.25£-12 7,52£-16 8,00£-14 2.00£-14 5.20£-17 2.00E-12 5.00E-13 3,47£-14 4.00£-12 l.OOE-12 7/2/1984 5.29£-16 5.00£-12 1.25£-12 6.18£-16 8,00£-14 2.00£-14 1.40£-16 2.00E-12 5.00£-13 1.32£-14 4.00£-12 l.OOE-12 10/1/1984 1.74£-16 5.00£-12 1.25£-12 7.10£-17 8.00£-14 2,00£-14 l.OOE-16 2.00£-12 5.00£-13 1.08E-14 4.00£-12 1.00E-12 1/2/1985 1.00E-17 S.OOE-12 1.25£-12 7.10£-17 B.OOE-14 2.00E-14 7.80E-17 2.00E·12 5.00E-13 2.73E-14 4.00E-12 1.00E-12 4/1/1985 1.00E-16 S.OOE-12 1.25£-12 2.76£-16 8.00£-14 2.00E-14 4.10£-17 2.00£-12 5.00£-13 1.12£-14 4.00£-12 1.00£-12 7/1/1985 1.04E-16 5.00£-12 1.25£-12 l.OOE-16 8.00£-14 2.00£-14 l.OOE-16 2.00£-12 5.00£-13 1.64E-14 4.00£-12 1.00E-12 9/30/1985 1.00£-16 5.00£-12 1.25£-12 l.OOE-15 S.OOE-14 2.00£-14 l.OOE-16 2.00£-12 5.00£-13 1.73£-14 4.00£-12 1,00£-12 1/2/1986 1.03£-15 S.OOE-12 1.25£-12 3.17E-16 S.OOE-14 2.00£-14 1.25£-16 2.00E·12 5.00£-13 1.21E-17 4.00E-12 1.00£-12 4/1/1986 8.04£-16 S.OOE-12 1.25£-12 1.93E-17 B.OOE-14 2.00E-14 1.54£-16 2.00E-12 5,00£-13 1.69£-14 4.00£-12 1.00E-12 6/30/1.9.86 4.29E-16 5.00E-12 1.25£-12 1.77E-16 8 OOE-14 2.00£-14 2.83E-16 2.00E·12 5.00E-13 1.97E-14 4,00E-12 l.OOE-12 10/27/1!}86 6.45E-16 S.OOE-12 L2SE·12 9.89E-17 B.OOE-14 2.00E-14 4.16£-15 2.00£-12 5,00E-13 1.64£-14 4.00E-12 1.00E-12 12/15/1986 1.31£-16 S.OOE-12 1.25E-12 O.OOE+OO 8.00£-14 2.00E-14 4.16£-17 2.00E·12 5.00E-13 4.60£-15 4.00£-12 l.OOE-12 3/16/1987 2.01E-16 5.00E-12 1.25E-12 1.20£-16 8.00£-14 2.00£-14 5.73£-17 2.00E·12 5.00£-13 1.60£-14 4.00£-12 l.OOE-12 5/11/1987 :2.16£-16 5.00E-12 1.25£-12 1.96E-16 8,00£-14 2.00£-14 7.38E-17 2.00E-12 5.00£-13 1.59£-14 4.00£-12 l.OOE-12 9/9/1987 2.41E-16 5.00£-12 1.25E-12 2.18E-16 8.00£-14 2.00£-14 3.52£-17 2.00E·12 5.00E-13 1.46E-14 4.00£-12 1.00E-12 11/2/1987 2.44£-16 5.00£-12 1.25£-12 2.32E-16 8.00E-14 2.00£-14 l.37E-17 2.00E·12 S.OOE-13 2.48E-14 4.00£-12 l.OOE-12 2/16/1988 8.08E-16 5.00E-12 1.25E-12 2.55E-16 8,00£-14 2.00E-14 3.42E-16 2.00E-12 S.OOE-13 S.61E-14 4.00E-12 1,00E-12 5/18/1988 1.14E-16 5.00E-12 1.25E-12 4.14E-17 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 5.00E-13 1.20E-14 4.00E-12 l.OOE-12 8/15/1988 2.08£-16 5.00E-12 1.25E-12 3.06E-16 8.00£-14 l.OOE-14 3.65£-17 2.00£-12 ~.OOE-13 1.36£-14 4.00E-12 l.OOE-12 11/14/1988 4.21£-16 S.OOE-12 1.25E-12 2.93£-16 8.00£-14 2.00£-14 1.09£-16 2.00£-12 5.00E-13 2.48£-14 4.00£-12 l.OOE-12 2/13/1989 4.45E-16 5.00E-12 1.25E-12 4.78E·17 8.00£-14 2.00E-14 2.47E-17 l.OOE-12 S.OOE-13 3.34£-14 4.00E-12 l.OOE-12 5/15/1989 1.05£-16 5.00£-12 1.25£-12 l.OOE-16 8.00E-14 2.00E-14 2.45£-17 2.00E·12 S.OOE-13 6.56£-15 4.00£-12 l.OOE-12 8/14/1989 1.31£-16 5.00£-12 1.25£-12 5.85E-17 8.00E-14 2.00£-14 3.97£-17 2.00E·12 5.00£-13 6.75E-15 4,00E·12 l.OOE-12 1.1/.13/19&9 1.67E-16 5.00E-12 1.25£-12 3.87E-17 8.00E-14 'Z.OOE-14 8.03E-17 2.00£-12 5.00E-13 1.69E-14 4.00£-12 l.OOE-12 2/12/1990 4.43£-16 S.OOE-12 1.25E-12 l.OOE-16 8.00E·14 z.OOE-14 3.50E-17 2.00£-12 5.00£-13 2.37£-14 4.00E-12 l.OOE-12 5/14/1990 3.84£-16 S,OOE-12 1.25E-12 2.54£-16 8.00£-14 2.00E-14 1,02£-16 2.00£-12 5.00E·13 1.68£-14 4.00E-12 l.OOE-12 'M13/1990 7.27E-17 S.OOE-12 1.25E-12 2.87E-16 8.00E-14 2.00£-14 1.21E-17 2.00E-12 5.00£-13 7.86£-15 4.00£-12 l.OOE-12 11/12/1990 1.84E-16 S.OOE-12 1.25E-12 1.34E-16 8.00E-14 2.00£-14 8.53£-17 2.00E·12 5.00E-13 2.01£-14 4.00£-12 l.OOE-12 2/11/1991 4.66E-17 5.00E-12 1.25E-12 8.48£-16 B.OOE-14 2.00£-14 1.94£-17 2.00E-12 5.00E·13 3.69£-14 4.00£-12 1,00E·12 5/13/1991 5.05E-17 5.00E-12 l.25E-12 7.40E-17 B.OOE-14 2.00E-14 7.00E-18 2.00E-12 5.00E-13 1.SOE·14 4.00E-12 l.OOE-12 8/12/1991 7.14£-17 5.00E-12 1.25E-12 6.22E-17 B.OOE-14 2.00E-14 7.95E-17 l.OOE-12 5,00E-13 1.77E-14 4.00E-12 l.OOE-12 11/11/1991 1.41E-17 5,00E-12 1.25£-12 2.19£-18 B.OOE-14 2.00E-14 2.75E-17 2.00£-12 5.00£-13 1.18£-14 4.00£-12 l.OOE-12 2/10/1992 8.12£-17 o.OOE-12 1.25£-12 2.35E-17 8.00£-14 2.00E-14 2.76E-18 2.00£-12 5.00E-13 3.57£-14 4.00£-12 1,00£-12 5/11/1992 9.18E-17 S,OOE-12 1.25E-12 5.80£-17 B.OOE-14 2.00£-14 3,36E-17 2.00£-12 5.00£-13 1.28£-14 4.00£-12 l.OOE-12 8/-10/1992 2.00E-18 S.OOE-12 l.25E-12 4.19E-17 B.OOE-14 2.00£-14 2.00£-18 2.00E-12 5.00£-13 1.59E-14 4.00£-12 1,00E-12 11/9/1992 4.00E-17 S.OOE-12 1.25£-12 2.68£-17 B.OOE-14 2.00£-14 1.07£-17 2.00E-12 5.00£-13 1.81£-14 4.00E-12 1.00£-12 2/9/1993 7.94E-17 S.OOE-12 1.25E-12 l.OOE-16 B.OOE-14 2,00£-14 1.09£-16 2.00E·12 5.00£-13 2.69E-14 4.00£-12 l.OOE-12 5/10/1993 1.60£-17 5.00E-12 1.25E-12 5.07£-17 B.OOE-14 2.00£-14 7.64£-17 2.00£-12 5.00E-13 1.26E-14 4.00£-12 l.OOE-12 8/J0/19'33' 6.00£-17 S.OOE-12 1.25E-12 6.00£-18 /3.00£-14 2.00£-14 l.OOE-16 2.00E-12 5.00£-13 1.50E-14 4.00£-12 1.00£-12 11/8/1993 l.OOE-16 S.OOE-12 1.25£-12 l.OOE-16 8.00E-14 2.00£-14 l.OOE-16 2,00E·12 5.00£-13 2.10£-14 4.00£-12 l.OOE-12 2/7/1994 1,61E-16 S.OOE-12 1.25£-12 1.00E-16 8.00E-14 2.00£-14 2.22E-16 .2.00£-12 S.OOE-13 2.23£-14 4.00£-12 l.OOE-12 5/9/1994 2.77£-16 S.OOE-12 1.25£-12 2.80£-17 8,00E-14 2.00£-14 8.37E-18 2.00£-12 S.OOE-13 1.40£-14 4.00£-12 l.OOE-12 8/9/1994 7.39E-17 5.00E-12 1,25E-12 l.OOE-16 8.00E-14 2.00£-14 1.14E-16 2.00E·12 5.00E-13 l.OOE-16 4.00£-12 l.OOE-12 11/7/1994 9.05£-17 5.00£-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 l.OOE-16 2.00E·12 5.00E-13 l.OOE-16 4.00£-12 l.OOE-12 Date Ufluent Concentration Limit= 9E-14 uCi/ml BHV-3U Effluent Concentration Limit= 2E-14 uCi/ml BHV-3T Effluent Concentration Limit= 9E-13 uCi/ml BHV-3R Effluent Concentration Limit= 6E-13 uCi/ml BHV-3PB ALARAGoal-2.25E-14 uCi/ml ALARAGoal = SE-13 uCi/ml .ALARA Goal = 2.2SE-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml Pre 1994 MPC Limit= SE-12 uCi/ml PrU9!i4 MPC Umll " SE-14 uCi/ml Pre 1994 MPC Limit= 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL-SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2}7/1995 7.99E-17 9.00E-14 2.25E·14 9.60E-17 2.00E-14 5.00E-15 9.60E-17 9.00E-13 2.25E-13 9 05E-15 6.00E-13 1.50E-13 5/9/1995 9.40E-17 9.00E-14 2.25E-14 9.80E-17 2.00E-14 5.00E-15 8.60E-17 9.00E-13 2.25E-13 2.88E-15 6.00E-13 1.SOE-13 8/9/1995 7.30E-17 9.00E-14 2.25E-14 9.20E-17 Z.OOE-14 5.00E-15 4.40E-17 9 OOE-13 2.25E-13 1.96E-15 6,00E-13 1.50E-13 U/U/1.9<J.S 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 2/5/1996 3.41E-16 ~.OOE-14 2.25E-14 2.26E-16 Z.OOE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6,00E-13 1.50E-13 5/6/1996 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 8/5/1996 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 .3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 l.l/6/1996 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 2/6/1997 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9,00E-13 2.25E-13 2.69E-14 G.OOE-13 1.50E-13 5/5/1997 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 8/11/1997 3.00E-16 9,00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 G.OOE-13 1.50E-13 1/5/1998 3,16E-16 9.00E-14 2.25E-14 1.31E-16 Z.OOE-14 5.00E-15 p.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 4/28/1998 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E·15 1.18E-16 9,00E-13 2.25E-13 Z.69E-14 6.00E-13 1.50E-13 7/31/1998 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6,00E-13 1.50E-13 9/28!1998 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9,00E-13 2.25E·13 1.31E-14 6.00E-13 1.50E-13 12/28/1998 3.16E-16 9,00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/29/1999 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5,00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/3/1999 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/27}1999 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1,31E-14 6.00E-13 1.50E-13 12/28/1999 3.16E-16 9.00E-14 2.25E-14 1.31E-16 ~.OOE-14 5.00E-15 6.58E-17 9,00E-13 2.25E-13 1,91E-14 6.00E-13 1.50E·13 3/28/2000 3.41E-16 9.00E-14 2.25E-14 2.26E-16 l.OOE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6,00E-13 1.50E-13 6/26/2000 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5,00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/26/2000 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/26/2000 3.16E-16 9.00E-14 2.25E-14 1.31E-16 Z.OOE-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/26/2001 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9,00E-13 2.25E-13 2.69E-14 6.00E-13 1,50E-13 7/2/2001 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/24/2001 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5,00E-15 3.99E-16 9,00E-13 2 25E-13 1.31E-14 6.00E-13 1.50E-13 12/31/2001. 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5,00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6,00E-13 1.50E-13 4/1/2002 3.41E-16 9.00E-14 2.25E-14 2.26E-16 Z.OOE-14 5.00E-15 l.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/1/2002 1.31E-16 9.00E-14 2.25E-14 1.39E-16 Z.OOE-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1,50E-13 9/3Q/2002 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 !3.DOE-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/30/2002 3.16E-16 9.00E·14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/31/2003 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E·13 2.69E-14 6,00E·13 1.50E-13 6/30/2003 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/29/2003 a.OOE-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 1.25E-13 1.31E-14 6.00E-13 1.50E-13 12/29/2003 3.16E-16 9.00E-14 2.25E-14 1,31E-16 2.00E-14 S.OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/29/2004 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2,00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 l.SOE-13 6/27/2004 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2,00E-14 S.OOE-15 1.82E-16 9.00E-13 2 25E-13 1.53E-14 6.00E-13 1.50E-13 9j27/2004 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6,00E-13 1.50E-13 12/27/2004 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 G.OOE-13 1.50E-13 3/28/2005 3,41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/29/2005 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 9/26/2005 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9,00E-13 2.25E-13 1.31E-14 6,00E-13 L50E-13 1/3/2006 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 01/3/2006 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5,00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/3f2oo6 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 10/2/2006 3.00E-16 9.00E-14 2.25E-14 3.43E-16 Z,OOE-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1,31E-14 6.00E-13 l .SOE-13 1/1/2006 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 S.OOE-15 6.58E-17 9.00E-13 2,25E-13 1.91E-14 6,00E-13 1.50E-13 4/2/2007 3.41E-16 ,.OOE-14 2,25E-14 2.26E-16 2,00E-14 5,00E-15 1.18E-16 9,00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/212007 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5,00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6,00E-13 1.50E-13 9/30/2007 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/31/2007 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2,00E-14 5.00E-15 p.58E-17 9 OOE-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 3/31/2008 3.41E-16 9.00E·14 2.25E-14 2.26E-16 Z.OOE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 6/30/2008 1.31E-16 9.00E-14 2,25E-14 1.39E-16 2.00E-14 S,OOE-15 1.82E-16 ~.OOE-13 2.25E-13 1.53E-14 6.00E-13 l.SOE-13 Date Effluent Concentration Limit-9E-14 uCi/ml 1!HV-3U Effluent Concentration Limit-ZE-14 uCi/ml BHV-3T Effluent Concentration Limit -9E-13 uCi}ml BHV-3R Effluent Concentration Limit-6E-13 uCi/ml BHV-3PB ALARAGoal-2.2SE-14 uCi/ml ALARAGoal-SE-13 uCi/ml ALARA Goal-2.25E-13 uCi/ml ALARA Goal -l.SE-13 uCi/ml Pre:19!14 MPC Limit= SE-12 uCi/ml Pre 1994 MPC Limit= BE-14 uCi/ml Pre 1994 MPC Limit= 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE·12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 G.OOE-13 1.50E-13 12/31/2008 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 S.OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 G.OOE-13 L50E-13 3/15/2009 3.41E-16 ·9.00E-14 2.25E-14 2.26E-16 2.00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 G.OOE-13 1.50E-13 6/15/2009 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 p.OOE-13 1.50E-13 9/15/2009 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-l3 1.31E-14 6.00E-13 1.50E-13 12/lS/2009 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 G.OOE-13 1.50E-13 3/31/2010 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 S.OOE-15 1.18E-16 9.00E-13 2,25E-13 2.69E-14 6.00E-13 1.50E-13 6/30/2010 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 G.OOE-13 1.50E-13 9/30/2010 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S,OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 12/31/2010 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 4/4/2011 3.41E-16 9.00E-14 2.25E-14 2.26E-16 Z.OOE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2,69E-14 6.00E-13 1.50E-13 7/4/2011 1.31E-16 S.OOE-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 10/3/2011 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5,00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.SOE-13 1/3/2012 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 L91E-14 6.00E-13 l.SOE-13 4/3/2012 3.41E-16 9.00E-14 2.25E-14 2.26E-16 Z.OOE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/2/2012 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 G.OOE-13 1.50E-13 10/1/2012 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5,00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 G.OOE-13 1.50E-13 12/31/2012 3.16E-16 9,00E-14 2.25E-14 1.31E-16 2.00E-14 S.OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 G.OOE-13 1.50E-13 3/25/2013 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13 7/2/2013 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S,OOE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 G.OOE-13 1.50E-13 9/30/2013 3.00E-16 9.00E-14 i.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 G.OOE-13 1.50E-13 12/30/2013 3.16E-16 9.00E-14 2.25E-14 1,31E-16 2.00E-14 S.OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 G.OOE-13 1.50E-13 3/31/2014 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 S.OOE-15 1.18E-16 9,00E-13 2.25E-13 2.69E-14 G.OOE-13 1.50E-13 6/30/2014 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 G.OOE-13 1.50E-13 -E -0 ::::J -en £: 0 ·~ -£: C1) () £: 0 (.) 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I•~ I•~ I•~ I•~ 14 f::: .. 14~ ~~ ~~ i4F: ~~ I•~ .~ • .:::: • ..! ~ ... ~ ~ ,, ~ I ~ioc: ?'II '<t lO .-w I UJ 0 0 0 0 ~are::ls 5olf 5: [: ~ ~ ~ ~ ~ ~ ~ ~ s: ~ ~ ~ ~ ~ 5! ~ 1 I .. ~ la ~ r-. ~ N ~ F::: F:: __., <D .- I UJ 0 ~ 1'-.- I UJ 0 ~ .- " - - - - - - - - - co .-I UJ 0 0 8~-das c~-das ~~-des o~-das 6o-das so-das Lo-des go-das so-das vo-das 8o-das co-das w-das oo-das 66-das B6·das L6·das 96-das S6-das v6-das 86-das c6·das ~6-das 06·das 6s-das ss-das Ls-das gs-das ss-das vs-das 8s-das cs-das ~s-das -:§ 0 :::J -Ill s:::: 0 ~ '--s:::: G> u s:::: 0 0 tO N N I E :::J "C co a: M > :I: [Q ,..,.. ..-C\1 ..-..-I I L.U L.U 0 0 C! C! ~ ..-: (V) """ LO ..-..-..-I I I L.U L.U L.U 0 0 0 C! 0 0 ..-~aiB:JS DOlf ,.. 1-~ F-..... F-.... ~r--.... f.. ~ ~i-.... i-~ ~c f:: .... ~r---.... r---.... i-.... r---.... ~;:::. I ~ '-. ..... -~ ::;:;;: .... ~::::: -~ -..... ,.j ~ • 4 ~ ,.... ' ~ ~ __. -..... ~-:::>+ co ..-I L.U 0 C! ..- __.,.. • :t • ..... ,....., ..-I L.U 0 C! ..- . ' - - - . - - - - co ..-I L.U 0 C! ..- 8~-das c~-das ~ ~-das o~-das 6o-das so-das La-das go-d as go-d as vo-das 8o-das c:m-das w-das oo-das 66-das 95-das L6-das 95-das 95-das 175-das 86-das c6-das ~5-das 05-das 6a-das se-d as La-das gg-das gg-das pg-das 8a-das ca-das ~g-das -E :::::: 0 ::::J -1/) t: 0 :,;:::; ca ... -t: Cl) CJ t: 0 0 0 ,.. C}l 'tJ ca Cl) ..J C") ::> J: Ill .-I w 0 0 C\1 C') .-I Li.J w 0 0 ~ ~ .- ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ltc: ~ ltc: ~ ltc: ~ ltc: ~ ltc: r..-ltc: ~ ltc: ~ ltc: ~ ltc: ~ ltc: ~ !«: ~ ~ ~ .ltc: ~ !«: i-i? , --~ ~ ~ F-~ Ito F:; I• ~ I'll ~ ~ ~==~---r+ fl._ ~ Ito= l5. I• I::: ~ ~ ~ • ...... "<:t .-I w 0 0 (aiBOS DOl) . I!) (() .- uJ I w 0 0 ~ ~ - - - - I'-.- I w 0 ~ .- 8~-das c::~-das ~ ~-das o~-das 6o-das so-das La-das go-d as so-das vo-das 8o-das c::o-das ~o-das oo-das 66-das 86-das L6-das 95-das 95-das 175-das 86-das <::6-das ~5-das 06-das 6s-das ss-das La-das gs-das ss-das vs-das 8s-das c::s-das ~s-das TAB4 BHV -4 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit= 9E-14 uCi/ml 'BHV-4U Effluent Concentration Limit-2E-14 uCi/ml BHV-4T Effluent Concentration Limit-9E-13 uCi/ml BHV-4R Effluent Concentration Limit= 6E-13 uC[/ml BHV-4PB ALARA Goal= 2.25E-14 uCi/ml ALARA Goal= SE-13 uCi/ml ALARA Goal= 2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre:·1994 MK limit = BE-14 uCi/ml Pre 1994 MPC Limit = 2E·12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL= :J..25E-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 A LARA GOAL= 1E-12 uCi/ml Cone EFC EFCA Cone HC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 5.20E-15 S.OOE-12 1.25E-12 2,93E-15 8.00E-14 2.00E-14 2.74E-15 2.00E-12 S.OOE-13 1,84E-14 4.00E-12 1.00E-12 12/14/1981 4.53E-15 S.OOE-12 1.25E-12 1.78E-15 B.OOE-14 2,00E-14 2.29E-15 2.00E-12 S.OOE-13 2.54E-14 4.00E-12 l.OOE-12 3/29/1982 1.06E-15 S.OOE-12 1.25E-12 1.42E-14 I!.OOE-14 2.00E-14 1.07E-15 2.00E-12 5.00E-13 2.31E-14 4.00E-12 l.OOE-12 6/30/1982 6,03E-15 S,OOE-12 1.25E-12 1.57E-14 s.OOE-14 2.00E-14 2.62E-15 2.00E-12 5.00E-13 2.25E-14 4.00E-12 l.OOE-12 9/27/1982 1.26E-14 5.00E-12 1.25E-12 7.58E-16 KOOE-14 2.00E-14 5.35E-15 2.00E-12 5.00E-13 2.68E-14 4.00E-12 l.OOE-12 1/3/1983 ,4.33E-15 5.00E-12 1.25E-12 6.52E-16 8.00E-14 2.00E-14 6.04E-16 2.00E-12 5,00E-13 2.57E-14 4.00E-12 l.OOE-12 4/4/1983 1.25E-15 S.OOE-12 1.25E-12 7.17E-16 8.00E-14 2.00E-14 6.76E-16 2,00E-12 5.00E-13 2.00E-14 4.00E-12 l.OOE-12 6/30/1983 3.73E-16 S.OOE-12 1.25E-12 9.43E-16 S.OOE-14 2.00E-14 4.13E-16 2,00E-12 5.00E-13 1,20E-14 4,00E-12 l.OOE-12 10/3/1983 2.54E-16 S.OOE-12 1.25E-12 1.51E-16 S.OOE-14 2.00E-14 2.6SE-16 2.00E-12 S.OOE-13 2.SOE-14 4.00E-12 l.OOE-12 1/3/1984 2.76E-15 5.00E-12 1.25E-12 1.60E-16 S.OOE-14 2.00E-14 l.OSE-16 2.00E-12 5.00E-13 1,59E-16 4.00E-12 1,00E-12 4/2/1984 ,4.27E-16 S.OOE-12 1.25E-12 2.33E-16 8.00E-14 2.00E-14 6.28E-16 2.00E-12 5.00E-13 3.67E-14 4.00E-12 l.OOE-12 7/2/1984 2.57E-15 S,OOE-12 1.25E-12 1.36E-16 8.00E-14 2.00E-14 1.11E-16 2.00E-12 5.00E-13 1.58E-14 4.00E-12 l.OOE-12 10/1/1984 4.18E-16 S.OOE-12 1.25E-12 3.54E-16 8.00E-14 2.00E-14 1.10E-17 2.00E-12 5.00E-13 9.83E-15 4.00E-12 l.OOE-12 1/2/1985 5.30E-17 5.00E-12 1,25E-12 3.55E-17 8.00E-14 2.00E-14 7.00E-18 2.00E-12 5.00E-13 2.57E-14 4.00E-12 l.OOE-12 4/1/1985 l.OOE-16 5.00E-12 1.25E-12 6.00E-16 8.00E-14 2.00E-14 I\.35E-17 2.00E-12 5.00E-13 5.02E-15 4.00E-12 l.OOE-12 7/1/1985 9.36E-16 5.00E-12 1.25E-12 2.33E-16 8.00E-14 2.00E-14 2.36E-16 2.00E-12 .S.OOE-13 7.48E-15 4.00E-12 l.OOE-12 9/30/1985 1.46E-15 S.OOE-12 1.25E-12 7,69E-16 8.00E-14 2.00E-14 5.38E-16 2.00E-12 5.00E-13 7.86E-15 4.00E-12 l.OOE-12 1/2/1986 8.40E-15 5.00E-12 1.25E-12 7.60E-16 8.00E-14 2.00E-14 2.99E-16 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 l.OOE-12 4/1/1986 5.79E-15 S.OOE-12 1.25E-12 5.80E-16 8.00E-14 2.00E-14 1.34E-15 2.00E-12 S.OOE-13 1.33E-14 4.00E-12 l.OOE-12 6/30/1986 5.19E-15 5.00E-12 1.25E-12 7.83E-16 8.00E-14 2.00E-14 2.20E-15 2.00E-12 5.00E-13 7.14E-16 4.00E-12 1.00E-12 10/27/1986 4.60E-15 5.00E-12 1.25E-12 4.67E-16 8.00E-14 2.00E-14 2.37E-15 2.00E-12 S.OOE-13 1.13E-14 4.00E-12 l.OOE-12 12/15/1986 2.75E-15 5.00E-12 1.25E-12 5.90E-16 8.00E-14 2.00E-14 9.39E-16 2.00E-12 5.00E-13 1.20E-14 4.00E-12 l.OOE-12 3/16/1987 4.64E-15 S.OOE-12 1.25E-12 1.18E-15 8.00E-14 2.00E-14 4.97E-16 2.00E-12 S.OOE-13 5,89E-14 4.00E-12 l.OOE-12 5/11/1987 4.35E-15 S.OOE-12 1.25E-12 1.23E-14 8.00E-14 2.00E-14 l.BE-15 2.00E-12 5.00E-13 l.21E-14 4.00E-12 1.00E-12 9/9/1987 6.39E-15 5.00E-12 1.25E-12 1.50E-14 8.00E-14 2.00E-14 2.26E-15 ,l.OOE-12 S.OOE-13 1.57E-14 4.00E-12 1.00E-12 11/2/1987 6.72E-15 S.OOE-12 1.25E-12 4.53E-16 8,00E-14 2.00E-14 2.20E-15 2.00E-12 S.OOE-13 .2.S5E-14 4.00E-12 l.OOE-12 2/16}1988 1.91E-15 5.00E-12 1.25E-12 1.35E-14 8.00E-14 2.00E-14 4.42E-16 2.00E-12 5.00E-13 4.44E-14 4.00E-12 1.00E-12 5/18/1988 1.78E-14 S.OOE-12 1.25E-12 4.39E-14 8.00E-14 2.00E-14 4.92E-16 2.00E-12 5.00E-13 1.38E-14 4.00E-12 l.OOE-12 8/15/1988 7.56E-15 S.OOE-12 1.25E-12 3.31E-14 S.OOE-14 2.00E-14 l .S1E-15 2.00E-12 5.00E-13 1.97E-14 4.00E-12 l.OOE-12 11/14/1988 1.47E-14 p.OOE-12 1.25E-12 1.56E-15 8.00E-14 2.00E-14 2.57E-15 2.00E-12 5.00E-13 2.12E-14 4.00E-12 l.OOE-12 2/13/1989 2.47E-15 S.OOE-12 1.25E-12 3.14E-15 S.OOE-14 2.00E-14 6.94E-16 2.00E-12 5.00E-13 2.12E-14 4,00E-12 l.OOE-12 5/15/1989 2.50E-16 s.OOE-12 1.25E-12 7.68E-15 8.00E-14 2.00E-14 9.03E-16 2.00E-12 5.00E-13 8.05E-15 4.00E-12 1.00E-12 8/14/1989 6.50E-15 S.OOE-12 1.25E-12 4.72E-15 8.00E-14 2.00E-14 2.35E-15 2.00E-12 5,00E-13 9.95E-15 4.00E-12 l.OOE-12 11/13/1989 9.63E-15 ,5.00E-12 1.25E-12 4.05E-15 8.00E-14 2.00E-14 4.03E-15 2.00E-12 S,OOE-13 1.99E-14 4.00E-12 l.OOE-12 2/12/1990 8.92E-15 S.OOE-12 1.25E-12 3.56E-15 B.OOE-14 2.00E-14 2.89E-15 2.00E-12 5.00E-13 2.69E-14 4.00E-12 l.OOE-12 5/14/1990 8.90E-15 5.00E-12 1.25E-12 3.58E-15 B.OOE-14 2.00E-14 2.33E-15 2.00E-12 5.00E-13 2,09E-14 4.00E-12 l.OOE-12 8/13/1990 1.92E-15 S.OOE-12 1.25E-12 1.87E-15 B.OOE-14 2.00E-14 5.06E-16 2.00E-12 5.00E-13 8.86E-15 4.00E-12 1,00E-12 11/12/1990 2.91E-15 5.00E-12 1.25E-12 2.25E-17 8.00E-14 2.00E-14 1.08E-15 2.00E-12 5.00E-13 2.19E-14 4.00E-12 l.OOE-12 2/11/1991 1.67E-16 5.00E-12 1.25E-12 7.89E-16 8.00E-14 2.00E-14 6.38E-17 2.00E-12 5.00E-13 4.19E-14 4.00E-12 l.OOE-12 5/13/1991 1.87E-16 5.00E-12 l.25E-12 2.61E-15 B.OOE-14 2.00E-14 3.54E-16 2.00E-12 5.00E-13 1.40E-14 !I.OOE-12 l.OOE-12 8/12/1991 4.85E-16 5.00E-12 1.25E-12 4.38E-16 B.OOE-14 2.00E-14 1.27E-16 2.00E-12 5.00E-13 2.20E-14 1\.00E-12 1.00E-12 11/11/1991 1.77E-16 S.OOE-12 1.25E-12 1.46E-16 8.00E-14 2.00E-14 3.76E-17 2,00E-12 S.OOE-13 1.15E-14 4.00E-12 l.OOE-12 2/10/1992 1.83E-16 5.00E-12 1.25E-12 1.95E-15 8,00E-14 2.00E-14 1.33E-16 2,00E-12 S.OOE-13 3.35E-14 4.00E-12 l.OOE-12 5/11/1992 4.40E-16 S.OOE-12 1.25E-12 ,2.S6E-16 S.OOE-14 2.00E-14 4.04E-16 2.00E-12 5.00E-13 1,41E-14 4.00E-12 l.OOE-12 8/10/1992 9.09E-17 5,00E-12 1.25E-12 1.15E-16 8.00E-14 2.00E-14 4.50E-17 2.00E-12 ,5.00E-13 1.57E-14 ii.OOE-12 l.OOE-12 11/9/1992 2.07E-16 5,00E-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 3,62E-17 2.00E-12 S.OOE-13 2.24E-14 4.00E-12 1,00E-12 2/9/1993 1.73E-16 S.OOE-12 1.25E-12 2.76E-17 8.00E-14 2.00E-14 2.89E-17 2.00E-12 S.OOE-13 3.08E-14 4.00E-12 l.OOE-12 5/10/1993 2.70E-17 5.00E-12 1.25E-12 2.50E-17 8.00E-14 2.00E-14 8.74E-17 2.00E-12 5.00E-13 l.25E-14 4.00E-12 l.OOE-12 8/10/1993 9.00E-17 5.00E-12 L25E-12 1.76E-16 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 5.00E-13 1.50E-14 4.00E-12 l.OOE-12 11/8/1993 l.OOE-16 5.00E-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 6.00E-17 2.00E-12 5.00E-13 1.75E-14 4.00E-12 l.OOE-12 2/7/1994 l.lOE-16 5.00E-12 1,25E-12 3.38E-16 8.00E-14 2.00E-14 2.21E-16 2.00E-12 5.00E-13 3.08E-14 4.00E-12 l.OOE-12 5/9/1994 3.80E-16 5.00E-12 1.25E-12 2.82E-16 8.00E-14 2.00E-14 3.46E-16 2.00E-12 5.00E-13 1.73E-14 4.00E-12 l.OOE-12 8/9/1994 3.85E-16 5.00E·12 1,25E-12 3.53E-16 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 S.OOE-13 l.OOE-16 4.00E-12 l.OOE-12 11/7/1994 6.21E-17 5.00E-12 1.25E-12 9.70E-17 8,00E-14 2.00E-14 1.96E-16 2.00E-12 S.OOE-13 l.OOE-16 4.00E-12 l.OOE-12 Date Effluent Concentration Limit = 9E-14 uCi}ml BHV-4U Effluent Concentration Limit -2E-14 uCi/ml BHV-4T Effluent Concentration Limit= 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB ALARAGoal= 2.25E-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal-2.25E-13 uCi/ml ALARAGoal-1.5E-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit= BE-14 uCi/ml Pre 1994 MPC Limit= 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 A LARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 A LARA GOAL= 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 3.70E-16 9.00E-14 2.25E-14 9.80E-17 2.00E-14 5.00E-15 9.70E-17 9.00E-13 2.25E-13 8.84E-15 p.OOE-13 1.50E-13 5/9/1995 9.40E-17 9.00E-14 2.25E-14 2.86E-16 2.00E-14 S.OOE-15 1.90E-16 9.00E-13 2.25E-13 2.90E-15 6.00E-13 1.50E-13 8/9/1995 1.45E-16 9.00E-14 2.25E-14 2.31E-15 2.00E-14 S.OOE-15 7.10E-17 9.00E-13 2.25E-13 2.70E-15 p.OOE-13 l.SOE-13 11/11/1995 1.43E-14 9.00E-14 2.25E-14 5.70E-15 2,00E-14 5.00E-15 2.61E-15 9.00E-13 .2.25E-13 S.60E-15 6.00E-13 1.50E-13 2/5/1996 1.19E-14 9.00E-14 2.25E-14 3.80E-16 2.00E-14 5.00E-15 6,10E-15 9.00E-13 2.25E-13 6.48E-15 p.OOE-13 1.SOE-13 5/6/1996 4.55E-16 9.00E-14 2.25E-14 3.57E-15 2.00E-14 S.OOE-15 2.84E-16 9.00E-13 2.25E-13 7.68E-15 6.00E-13 1.50E-13 8/5/1996 7.78E-16 9.00E-14 2.25E-14 3.51E-15 2.00E-14 .5.00E-15 1.69E-16 9.00E-13 2.25E-13 4.90E-15 6.00E-13 1.50E-13 11/6/1996 1.36E-15 9.00E-14 2.25E-14 1.00E-16 Z.OOE-14 5.00E-15 4.21E-16 9.00E-13 ,2.25E-13 l.lOE-14 G.OOE-13 1.50E-13 2/6/1997 l.OOE-16 9.00E-14 2.25E-14 1.40E-16 Z.OOE-14 5.00E-15 1.03E-16 9.00E-13 .2.25E-13 6.76E-15 6.00E-13 1.50E-13 5/5/1997 l.OOE-16 9.00E-14 2.25E-14 4,00E-16 2.00E-14 5.00E-15 2.24E-16 9.00E-13 2.25E-13 4.55E-15 6.00E-13 1.SOE-13 .8/11/1997 4.74E-16 9.00E-14 2.25E-14 9.07E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.55E-15 6.00E-13 1.50E-13 1/5/199.8 8-31E-16 9.00E-14 2.25E-14 4 . .82E-16 2.00E-14 5,00E-15 1.77E-16 9.00E-13 2.25E-13 5.28E-15 6.00E-13 1.50E-13 4/2.8/199.8 3.32E-16 9.00E-14 2.25E-14 4.43E-15 Z.OOE-14 5,00E-15 1.21E-16 9.00E-13 2.25E-13 7.43E-15 6.00E-13 1.50E-13 7/31/1998 4.60E-16 9.00E-14 2.25E-14 9.02E-16 Z.OOE-14 5.00E-15 3.54E-16 9.00E-13 2,25E-13 6.91E-15 6.00E-13 1,50E-13 9/28/1998 4.08E-16 9.00E-14 2.25E-14 4,93E-16 Z.OOE-14 5.00E-15 2,53E-16 9.00E-13 2.25E-13 4.52E-15 6.00E-13 1.50E-13 12/28/1998 7.72E-16 9.00E-14 .2.25E-14 3.75E-16 2.00E-14 5.00E-15 3.43E-16 9.00E-13 2.25E-13 6.73E-15 6.00E-13 1.50E-13 3/29/1999 5.11E-16 9.00E-14 .2.25E-14 4.70E-16 ,2.00E-14 5.00E-15 3.70E-16 9.00E-13 2,25E-13 8.96E-15 6.00E-13 1.50E-13 7/3/1999 5.90E-16 9.00E-14 2.25E-14 9.89E-16 2.00E-14 S.OOE-15 1.28E-16 9.00E-13 2.25E-13 6.40E-15 6.00E-13 1.50E-13 9/27/1999 1.70E-15 9.00E-14 2.25E-14 7.50E-16 .Z.OOE-14 S.OOE-15 4.61E-16 9.00E-13 2.25E-13 7.86E-15 6.00E-13 1.50E-13 12/28/1999 1.03E-15 9.00E-14 2.25E-14 7.50E-16 2.00E-14 5.00E-15 2.43E-16 9.00E-13 2.25E-13 6.42E-15 6.00E-13 l.SOE-13 3/27/2000 LOOE-16 9.00E-14 2.25E-14 2.13E-16 2.00E-14 5.00E-15 2.20E-16 9.00E-13 2.25E-13 5.61E-15 6,00E-13 1.50E-13 6/26/2000 1.75E-16 9.00E-14 2.25E-14 3.08E-16 2.00E-14 S.OOE-15 l.llE-16 9.00E-13 2.25E-13 3.92E-15 6.00E-13 1.50E-13 9/26/2000 3.65E-16 9.00E-14 2.25E-14 2.01E-16 2.00E-14 S.OOE-15 2.24E-16 ~.OOE-13 2.25E-13 7.79E-15 6.00E-13 1.50E-13 12/26/2000 2.27E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 4.35E-16 ~.OOE-13 Z.25E-13 8.45E-15 6.00E-13 1.SOE-13 3/26/2001 1.45E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 p.37E-15 6.00E-13 1.50E-13 7/2/2001 l.OOE-16 9.00E-14 2.25E-14 1.05E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.99E-15 6.00E-13 1.50E-13 9/24/2001 1.91E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 2.01E-16 9.00E-13 Z.25E-13 B.04E-15 6.00E-13 1.50E-13 12/31/2001 1.38E-16 9.00E-14 2.25E-14 2.05E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.83E-15 6.00E-13 1.50E-13 4/1/2002 2.20E-16 9.00E-14 2.25E-14 3.38E-16 2100E-14 5.00E-15 1.26E-16 9.00E-13 2.25E-13 7.48E-15 6.00E-13 1.50E-13 7/1/2002 1.97E-16 9.00E-14 2.25E-14 4,10E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.40E-15 6.00E-13 1.50E-13 9/30/2002 230E-16 9.00E-14 2.25E-14 2.42E-16 2.00E-14 5.00E-15 1.56E-16 9,00E-13 2.25E-13 4.21E-15 6.00E-13 1.50E-13 12/30/2002 l.OOE-16 9.00E-14 z.25E-14 1.92E-16 Z.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 9.42E-15 6.00E-13 1.SOE-13 3/31/2003 2.SOE-16 ~.OOE-14 .2.25E-14 1,69E-16 Z.OOE-14 5.00E-15 1.29E-16 9.00E-13 Z.25E-13 4.55E-15 6.00E-13 1.50E-13 6/30/2003 l.OOE-16 9.00E-14 2.25E-14 2.87E-16 z.OOE-14 5.00E-15 1,00E-16 9.00E-13 2.25E-13 4.20E-15 6.00E-13 1.50E·13 9/29}2003 1.00E-16 9.00E-14 2.25E-14 B.53E-16 2.00E-14 5.00E-15 3.32E-16 9.00E-13 2.25E-13 8.69E-15 6,00E-13 1.50E-13 12/29/2003 1.02E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.49E-15 9,00E-13 2.25E-13 9.45E-15 6.00E-13 1.50E-13 3/29/2004 1.00E-16 9.00E-14 2.25E-14 1.26E-16 Z,OOE-14 5.00E-15 1.00E-16 9.00E-13 2.Z5E-13 2,00E-15 6.00E-13 L50E·13 6/27/2004 1.00E·16 9.00E-14 2.25E-14 .2.53E·16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E·13 3.23E-15 p.OOE-13 1.50E-13 9/27/2004 1,00E-16 9,00E-14 2.25E-14 1.15E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 9.68E-15 6.00E-13 1.50E-13 12/27/2004 l.OOE-16 9.00E-14 2.25E-14 2.30E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.Z5E-13 1.37E-14 6.00E-13 1.50E·13 3/28/2005 1.00E-16 9.00E-14 Z.25E-14 2.66E-16 2,00E-14 5.00E-15 3.15E-16 9.00E-13 Z.Z5E-13 9.22E-15 6.00E-13 1.50E·13 6/29/2005 1.47E·16 9.00E-14 2.25E-14 1.45E·15 2.00E-14 5.00E·15 1.42E-16 9.00E-13 2.25E-13 9.34E-15 6.00E-13 1.SOE·13 9/26/2005 2.01E-16 9.00E-14 2.25E-14 2,06E-16 2.00E-14 S.OOE-15 4,80E-16 9.00E-13 2.25E-13 2.12E-14 6.00E-13 1.50E·13 1/3/2006 4.54E-16 9.00E-14 2.25E-14 1.24E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E·13 3.60E-14 ~.OOE-13 1.50E-13 4/3/2006 1.99E-16 9.00E-14 2 25E-14 1.32E·16 2.00E-14 .S.OOE-15 l.OOE-16 9.00E-13 2.Z5E-13 8.36E-15 6.00E-13 1.50E-13 7/3/2006 2.76E-16 9.00E-14 2.25E-14 2.63E-16 2.00E-14 5.00E-15 l.OOE-16 ll.OOE-13 Z.25E·13 1.03E-14 6.00E-13 l.SOE-13 10/2/2006 4.97E-16 9.00E-14 2.25E-14 2.37E·16 2-00E-14 5.00E·15 l.OOE-16 9.00E-13 2.25E-13 1,60E,14 6.00E-13 1.50E-13 1/1/2007 6.46E-16 9.00E-14 2.25E-14 2.81E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 2.10E-14 6.00E-13 1.50E-13 4/2/2007 7.08E-16 '9.00E-14 2.25E-14 3.20E'-16 2.00E-14 5.00E·15 l.OOE-16 9.00E-13 2.25E-13 1.54E-14 6.00E-13 1.50E-13 7/2/2007 9.41E-16 9.00E-14 2.25E-14 1.46E-16 2.00E-14 5.00E-15 1.99E-16 9.00E-13 2.25E-13 2.56E-14 6.00E-13 1.SOE-13 9/30/2007 3.30E-16 9.00E-14 2.25E-14 5.50E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.57E-15 6.00E-13 1.50E-13 12/31/2007 1.42 E-15 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9,00E-13 2 25E-13 9.93E-15 6.00E-13 1.50E-13 3/31/2008 1.25E·16 9.00E-14 2 25E-14 1.72E-16 2.00E-14 5.00E·15 l.OOE-16 9.00E-13 2.25E-13 4"09E-15 6.00E-13 1.50E-13 6/30/2008 1.28E-15 9.00E-14 Z.25E-14 l.OOE-16 2.00E-14 S.OOE-15 3,61E-16 9,00E-13 2.Z5E-13 1.18E-14 6.00E-13 1.50E-13 - Date ~ffluent Concentration Limit= 9E-14 uCi/ml BHV-4U Effluent Concentration Limit= 2E-14 uCi/ml BHV-4T Effluent Concentration Limit= 9E-13 uCi/ml 1!HV-4R Effluent Concentration Limit = ,GE-13 uCi/ml BHV-4PB I ALARAGoal = 2.25E-14 uCi/ml ALARA Goal= SE-13 uCi/ml ALARA Goal-2.25E-13 uCi/ml ALARA Goal= l.SE-13 uCi/ml I pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC Limit= BE-14 uCi/ml P.rl! 1994 MP<! Umlt-" 2E-12 uCi/ml Pr~ 1994 M PC _If mit~ 4E-12 uCi/ml Pre 1994 ALARA GOAL-1.25E-12 uCi/ml pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml f=onc EFC EFCA Cone EFC EFCA Cone EFC EFCA tone EFC EFCA 9/30/2008 2.72E-15 9.00E-14 2.25E-14 1.27E-15 2.00E-14 5.00E-15 '7.66E-16 9.00E-13 2.25E-13 1,10E-14 G.OOE-13 1.SOE-13 12/31/2008 2.88E-15 9.00E-14 2.25E-14 1.10E-15 2.00E-14 5.00E-15 6.56E-16 9.00E-13 2.25E-13 1.38E-14 G.OOE-13 1.50E-13 3/15/2009 1.56E-15 9.00E-14 2.25E-14 4.57E-16 2.00E-14 5.00E-15 2.99E-16 9.00E·13 2,25E-13 4.97E-15 G,OOE-13 1.50E-13 6/15/2009 5.67E-17 9.00E-14 2.25E-14 2.17E-16 z.OOE-14 5.00E-15 1.51E-16 9.00E-13 2.25E-13 4.47E-15 G.OOE-13 1.50E-13 9/15/2009 4.05E-15 9.00E-14 2.25E-14 1.45E-15 2.00E-14 5.00E-15 2.52E-16 9.00E-13 2.25E-13 1.24E-14 G.OOE-13 1.50E-13 I 12/15/2009 6.50E-15 9.00E-14 2.25E-14 3.48E-16 Z.OOE-14 5.00E-15 1,33E·16 9.00E·13 2.25E-13 7.60E-15 G.OOE-13 1.50E-13 3/31/2010 6.01E-15 9.00E-14 2.25E-14 1.26E-16 l.OOE-14 5.00E-15 1.34E-16 9.00E-13 2.25E·13 1.19E·14 G.OOE-13 1.50E-13 6/30/2010 2.33E-15 9.00E-14 ,2.25E-14 7.29E-16 l.OOE-14 5.00E-15 2.66E-16 9.00E-13 2.25E-13 3.27E-15 6.00E-13 1.50E-13 9/30/2010 4.77E-15 9.00E-14 2.25E-14 1.80E-15 2.00E-14 5.00E-15 8.23E-16 9.00E-13 2.25E-13 5.11E-15 G.OOE-13 1.50E-13 12/31/2010 3.93E-15 9.00E-14 2.25E-14 3,90E-16 Z.OOE-14 5.00E-15 2.56E-16 9.00E-13 2.25E-13 1,13E-14 G.OOE-13 1.50E-13 4/4/2011 1.29E-15 9.00E-14 2.25E-14 1.40E·16 2.00E-14 S.OOE-15 1,58E-16 ~.OOE-13 2.25E-13 1.11E-14 6.00E-13 1.50E-13 7/4/2011 3,30E-15 9.00E-14 2.25E-14 5.44E-16 2.00E-14 S.OOE-15 4.18E-16 S.OOE-13 2.25E-13 8.26E-15 6.00E·13 1.50E-13 10/3/2011 1.32E-15 9.00E-14 2.25E-14 7.89E-16 2.00E-14 5.00E-15 1.28E-16 S.OOE-13 2.25E-13 1.18E-14 G.OOE-13 1.50E-13 1/3/2012 1.04E-15 9.00E-14 2.25E-14 3.25E-16 2,00E-14 S.OOE-15 .2.28E-16 9.00E-13 2.25E-13 1.14E-14 G.OOE-13 1.50E-13 4/3/2012 ,2,51E-15 9.00E-14 2.25E-14 5.02E-16 2.00E-14 5.00E·15 2.27E-16 S.OOE-13 .2.25E-13 1.03E-14 G.OOE-13 1.50E·13 7/2/2012 2.62E-15 9.00E-14 2.25E-14 1.23E-15 2.00E-14 5.00E-15 2.97E-16 9.00E·13 2.25E-13 9.27E-15 6.00E-13 1.50E-13 10/1/2012 4.05E-15 9.00E-14 2.25E-14 8,33E-16 2.00E-14 5.00E-15 5.43E-16 9.00E-13 2.25E-13 l.21E-14 6.00E-13 1.50E·13 12/31/2012 2.32E-15 9.00E-14 2.25E-14 5.89E-16 2.00E-14 5.00E-15 3.75E-16 9.00E-13 2.25E-13 1.56E-14 6.00E-13 1.50E-13 3/25/2013 3.04E-15 9.00E-14 2.25E-14 4.99E·16 2.00E-14 5.00E-15 2.79E-16 9.00E-13 2.25E-13 2.13E-14 G.OOE-13 1.50E-13 7/2/2013 2.50E-15 9.00E-14 2.25E-14 3.62E·16 2.00E-14 5.00E-15 2.40E-16 9.00E-13 2.25E·l3 4.93E-15 G.OOE-13 1.50E-13 9/30/2013 2.98E-15 9.00E-14 2.25E-14 4.49E·16 Z.OOE-14 S.OOE-15 154E-16 9.00E·13 2.25E-13 7.49E·15 6.00E·13 1.50E·13 12/30/2013 3.88E-15 ll.OOE-14 2.25E-14 1.03E-16 Z.OOE-14 5.00E-15 4.47E-17 9.00E-13 2.25E-13 2.93E-14 6.00E-13 1.50E-13 3/31/2014 4,69E-15 9.00E-14 .2.25E-14 1.37E-16 2.00E-14 S.OOE-15 3.53E-16 9.00E-13 2.25E-13 l.OBE-14 6.00E-13 1.50E·13 6/30/2014 4.16E-15 9.00E-14 2.25E-14 6.96E-16 .Z.OOE-14 S.OOE-15 1.77E-15 9.00E-13 2.25E-13 LOGE-14 6.00E-13 1.50E-13 Sep-81 Sep-82 Sep-83 Sep-84 Sep-85 Sep-86 + Sep-87 c Sep-88 ...... 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C\1 I "'0 m Cl) ..J o::t :> :I: m T""'" ' w 0 ~ T""'" C\1 C') T""'" T""'" ' ' w w 0 0 ~ ~ T""'" ~ ~ ~ .. ..-....... ~ ,...lOt : ., ~ 191: ~ ~ .-:N ..__ «:; "'4~ ~ ~ i::>o p~ ~ ~ • ~ ... t ~ i< ~ ~ ~ • 0::::: ~ [~0::: ~ ::::. r-. > ~ ~ ~~ ~ ,.. ..., ~c::::.:.... ,_ > ~ II ~ ~ "<:t T""'" ' w 0 0 (areos flo1) • ..... 1.0 <0 T""'" T""'" ' ' w w 0 0 ~ ~ T""'" T""'" . . - ~ - - - - I'- T""'" ' w 0 ~ T""'" 8~-das c::~-das ~ ~-das o~-das 6o-das so-das Lo-das go-d as so-das to-das 8o-das c::o-das ~o-das oo-das 66-das 95-das L6-das 95-das 95-das t6-das 86-das <::6-das ~5-das 05-das 6s-das ss-das Ls-das gs-das ss-das ts-das 8s-das c::s-das ~s-das TABS BHV-5 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-SU Effluent Concentration Limit= 2E-14 uCi/ml BHV-ST Effluent Concentration limit= 9E-13 uCijml BHV-SR Effluent Concentration Limit = 6E-13 uCi/ml BHV-SPB AlARAGoal = 2.25£-14 uCi/ml AlARA Goal= SE-13 uCi/ml AlARAGoal = 2.25£-13 uCi/ml AlARAGoal = 1.5£-13 uCi/ml Pre 1994 MPC Limit-SE-UuCi/ml Prel994 MPC.Limfl; BE-14 uCi/ml Pre 1994 MPC Limit -2E-12 uCi/ml Pre 1994 MPC Limit-4E-12 uCi/ml Pre 1994 A lARA GOAL = l.25E-12 uCi/ml Pre 1994 A lARA GOAL = SE-13 uCi/ml Pre 1994 A lARA GOAL= 1E-12 uCi/ml Cone EFC eFCA Cone eFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 2.44E-15 S,OOE-12 1.25E·12 1.53E-15 8.00E-14 2.00E-14 7.54E-16 2.00E-12 5.00E-13 1.69E-14 4.00E-12 1.00E-12 12/14/1981 4,84E-15 S.OOE-12 1.25E-12 2.78E-15 8.00E-14 2.00E-14 1.84E-15 2.00E-12 5.00E-13 1.53E-14 4.00E-12 l.OOE-12 3/29/1982 1.04E-15 5.00E-12 1.25E-12 2.62E-15 8.00E-14 Z.OOE-14 1.11E-15 2.00E-12 5.00E-13 2.98E-14 4.00E-12 l.OOE-12 6/30/1982 3.61E-15 5.00E-12 1.25E-12 7.61E-15 S.OOE-14 2.00E-14 1.39E-15 2.00E-12 5.00E-13 1.80E-15 4.00E-12 l.OOE-12 9/27/1982 1.71E-14 5.00E-12 l.25E-12 9.46E-15 B.OOE-14 2.00E-14 3.80E-15 2.00E-12 5.00E-13 2.35E-14 4.00E-12 l.OOE-12 1/3/1983 1.90E-14 5.00E-12 125E-12 5.77E-15 S.OOE-14 2.00E-14 9.34E-17 2.00E-12 5,00E-13 4.32E-14 4.00E-12 l.OOE-12 4/4/1983 5.00E-12 1.25E-12 2.33E-15 B.OOE-14 2.00E-14 5.93E-16 2.00E-12 5.00E-13 3.01E-14 4.00E-12 l.OOE-12 6/30/1983 7.62E-16 5.00E-12 1.25E-12 3.25E-15 8.00E-14 Z.OOE-14 6.28E-15 2.00E-12 5.00E-13 2.69E-14 4.00E-12 l.OOE-12 10/3/1983 4.86E-16 5.00E-12 1.25E-12 L10E-15 S.OOE-14 2.00E-14 3.63E-16 2.00E-12 5.00E-13 2.08E-14 4.00E-12 l .OOE-12 1/3/1984 6.96E-15 5.00E-12 1.25E-12 9.69E-16 B.OOE-14 2.00E-14 9.60E-16 2.00E-12 5.00E-13 1.83E-14 4.00E-12 l.OOE-12 4/2/1984 1.64E-15 5.00E-12 1.25E-12 1.34E-15 8.00E-14 2.00E-14 3.88E-15 2.00E-12 5.00E-13 4.67E·14 4.00E-12 1.00E-12 7/2/1984 1.12E·15 5.00E·12 1.25E-12 1.92E-15 8.00E-14 2.00E-14 3.31E-15 2.00E-12 5.00E-13 2.21E·14 ·4.00E-12 l.OOE-12 10/1/1984 1.11E-15 5.00E-12 1.25E-12 3.13E-16 8.00E-14 2.00E-14 4.21E-16 Z.OOE-12 5.00E-13 1.57E-14 4.00E-12 l.OOE-12 1/2/1985 7.32E-16 5.00E-12 1.25E·12 6.71E-16 8.00E·14 2.00E-14 4..94E-16 2.00E-12 5.00E-13 2.42E-14 4.00E-12 l.OOE-12 4/1/1985 2.36E·16 5.00E-12 1.25E-12 5.43E-16 8.00E·14 2.00E-14 2.71E-16 2.00E-12 5.00E-13 1.25E-14 4.00E-12 1.00E-12 7/1/1985 7.58E-16 5.00E-12 1.25E-12 4.00E-16 8.00E-14 2.00E-14 6.90E-16 2.00E-12 5.00E-13 2.15E-14 4.00E-12 l.OOE-12 9/30/1985 7.47E·15 5 OOE-12 1.25E-12 1.16E-15 8.00E·14 Z.OOE-14 2.19E-15 Z.OOE-12 5.00E-13 9.20E-15 4.00E-12 l.OOE-12 1/2/1986 1.75E-14 5.00E-12 1.25E-12 7.24E-15 8.00E-14 2.00E-14 3.83E-15 2.00E-12 S.OOE-13 1.13E-16 4.00E-12 l.OOE-12 4/1/1986 2.99E·14 5.00E-12 1.25E-12 7.64E-15 8.00E-14 2.00E-14 1.51E-14 Z.OOE-12 S.OOE-13 2.22E-14 4.00E-12 l.OOE-12 6/30/1986 2.23E·14 5.00E-12 1,25E-12 5.19E-15 8.00E-14 2.00E-14 1.05E-14 2.00£-12 S.OOE-13 2.16E·14 4.00E-12 l.OOE-12 10/27/1986 2.33E-14 5.00E-12 1.25E-12 7.78E-15 8.00E-14 Z.OOE-14 1.60E-14 2 OOE-12 S.OOE-13 2.02E·14 4.00E-12 l .OOE-12 12/15/1986 3.40E·14 5.00E-12 1.25E-12 5.35E-15 8,00E-14 2.00E-14 1.47E-14 Z.OOE-12 o.OOE-13 2.82E-14 4.00E-12 l.OOE-12 3/16/1987 2.06E·14 5.00E-12 1.25E·12 4.SOE-15 8.00E-14 2.00E-14 6.74E-15 2.00E-12 S.OOE-13 7,29E·14 4.00E-12 1.00E-12 5/11/1987 2.50E-14 5.00E-12 1.25E-12 8.54E-15 8.00E-14 z.OOE-14 8.15E-15 Z.OOE-12 S.OOE-13 3.28E-14 4.00E-12 1.00E·12 9/9/1987 2.65E-14 5.00E-12 1.25E-12 6,62E-15 8,00E-14 2.00E-14 9.34E-15 2.00£-12 5.00E-13 2.77E·14 4.00E-12 l.OOE-12 11/2/1987 1.80E·14 5,00E-12 1.25E-12 7.09E-15 8.00E·14 2.00E-14 7.20E-15 ~.OOE-12 S.OOE-13 1.77E-14 4.00E-12 l.OOE-12 2/16/1988 1.01E-14 5.00E-12 1.25E-12 2.98E-15 B.OOE-14 2.00E-14 3,93E-15 2.00E-12 S.OOE-13 3.36E-14 4.00E-12 1.00E·12 5/18/1988 1.78E-14 5.00E-12 1.25E-12 8.14E-15 8.00E-14 Z.OOE-14 7.43E-15 Z.OOE-12 S.OOE-13 2.12E-14 4.00E-12 1.00E-12 8/15/1988 1.79E-14 5.00E-12 1.25E-12 1.49E-14 B.OOE-14 2.00E-14 5.34E-15 2.00E-12 ,S,OOE-13 2.45E-14 4.00E-12 1.00E-12 11/14/1988 4.46E·14 S.OOE-12 1.25E-12 1.39E-14 B.OOE-14 ~.OOE-14 1.17E-14 ,Z.OOE-12 5.00E-13 3.43E-14 4.00E-12 1.00E-12 2/13/1989 1.67E-14 S.OOE-12 1.25E-12 5.54E-15 B.OOE-14 2.00E-14 7.20E-15 Z,OOE-12 5.00E-13 5.02E-14 4.00E-12 1.00E-12 5/15/1989 2.03E-14 S.OOE-12 1.25E-12 7.05E-15 8.00E-14 2.00E-14 9.56E-16 .Z.OOE-12 S.OOE-13 l.43E-14 4.00E-12 1,00E-12 8/14/1989 2.81E-15 S.OOE-12 1.25E-12 3.78E-15 8.00E-14 2.00E-14 9.26E-15 l .OOE-12 G.OOE-13 1.50E-14 4.00E-12 l,OOE-12 11/13/1989 5.38E-14 5.00E-12 1.25E-12 8.01E·15 8.00E·14 2.00E-14 1.81E-14 2.00E·12 5.00E-13 4,09E·14 4.00E-12 1,00E-12 2/12/1990 4.48E·14 S.OOE-12 1.25E-12 1.48E·14 8.00E·14 2.00E-14 1.28E-14 2.00E-12 ·s.OOE-13 3.88E·14 4.00E-12 1.00E-12 5/14/1990 2.18E·14 5.00E-12 1.25E-12 1.70E-14 8.00E·14 2.00E-14 L59E-14 2.00E-12 S.OOE-13 3.49E·14 4.00E-12 1.00E-12 8/13/1990 9.53E·15 5.00E-12 1.25E-12 1,70E-14 8,00E-14 2.00E-14 3.27E-15 2.00E-12 S.OOE-13 1,27E·14 4.00E-12 1.00E·12 11/12/1990 1.11E-14 5.00E-12 1.25E-12 5.27E-15 8.00E-14 2.00E-14 5.38E-15 Z,OOE-12 5.00E-13 1.56E-14 4.00E-12 l.OOE-12 2/11/1991 6.35E-16 S.OOE-12 1.25E-12 3.13E-16 8.00E-14 2.00E-14 2.31E-16 2.00E-12 5.00E-13 3.89E-14 4.00E-12 1.00E·12 5/13/1991 1.22E·15 5.00E-12 1.25E-12 6.14E-15 8.00E-14 2.00E-14 4.41E-15 2.00E-12 5.00E-13 2.50E-14 4.00E-12 l.OOE-12 8/12/1991 7.84E·16 5.00E-12 1.25E-12 1.43E-15 B.OOE-14 2.00E-14 4.47E-16 2.00E-12 5.00E-13 1.84E-14 4.00E-12 l.OOE-12 11/11/1991 5.37E-16 5.00E-12 1.25E-12 4.20E-16 B.OOE-14 2.00E-14 1.37E-16 2.00E-12 5.00E-13 1.27E·14 4.00E-12 l.OOE-12 2/10/1992 3.54E·16 5.00E-12 1.25E·12 1.18E-16 B.OOE-14 2.00E-14 4.08E-17 2.00E-12 5.00E-13 3.69E·14 4.00E-12 l.OOE-12 5/11/1992 4.71E·16 5.00E-12 1.25E·12 9.58E-16 B.OOE-14 2,00E-14 8.31E-17 2.00E-12 5.00E-13 1.43E-14 4.00E-12 l.OOE-12 8/10/1992 5.32E·15 S.OOE-12 1.25E·12 3.36E-16 B.OOE-14 2.00E-14 1.65E-16 2.00E-12 5.00E-13 1.59E-14 4.00E-12 l.OOE-12 11/9/1992 3.66E-16 S.OOE-12 1.25E-12 2.25E-16 8.00E-14 2.00E-14 1.08E-16 2.00E-12 5.00E-13 2.24E·14 4.00E-12 l.OOE-12 2/9/1993 2.05E-16 S.OOE-12 1.25E-12 9.14E·17 8.00E-14 2.00E-14 6.31E-17 2.00E-12 5.00E-13 3.41E-14 4.00E-12 l.OOE-12 5/10/1993 4.80E·16 5.00E-12 1.25E-12 8.25E·16 8.00E·14 2,00E-14 1.26E-15 2.00E-12 5.00E-13 1.83E-14 4.00E-12 l.OOE-12 8/10/1993 8.30E-16 S.OOE-12 1.25E-12 1.90E-16 S.OOE-14 2.00E·14 2.10E-16 2.00E-12 5.00E-13 1.70E-14 4,00E-12 1.00E·12 11/8/1993 2.70E·16 5.00E-12 1.25E-12 8.00E-17 B.OOE-14 2,00E-14 7.00E-17 2.00E-12 S.OOE-13 2.34E-14 4.00E-12 '1.00E·12 2/7/1994 3.18E-16 S.OOE-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 5.18E-16 2,00E-12 5.00E·13 3.64E·14 4.00E-12 1.00E·12 5/9/1994 1.80E-15 5.00E-12 1.25E-12 9.78E-16 B.OOE-14 2.00E-14 l.lOE-15 2.00E·12 S.OOE-13 8.30E-15 4,00E-12 l.OOE-12 8/9/1994 2.67E-15 S.OOE-12 1.25E-12 l.11E-15 S,OOE-14 2.00E-14 4.95E-16 2.00E-12 5.00E-13 l.OOE-16 4.00E-12 l.OOE-12 11/7/1994 9.21E-17 5.00E-12 l.25E-12 1.59E-15 B.OOE-14 2.00E-14 1.66E-15 2.00E-12 S,OOE-13 l.OOE-16 4.00E-12 l.OOE-12 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-SU ~ffluent Concentration Limit = ZE-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit= 6E-13 uCi/ml BHV-SPB ALARA Goal= Z.ZSE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal= Z.ZSE-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml Pre 1994 MPC Limit= SE-12 uCi/ml pre 1994 MPC Limit = BE-14 uCi/ml Pre 1994 MPC Limit-ZE-12 uCi/ml Pre 1994 MPC Limit -4E-12 uCi/ml Pre 1994 ALARA GOAL= l.ZSE-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 A LARA GOAL -1E-12 uCi/ml Cone EFC EFCA tone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 1.51E-15 9.00E-14 2.25E-14 il.SOE-16 2.00E-14 S.OOE-15 9.70E-17 9.00E-13 2.25E-13 9.35E-15 6 OOE-13 1.50E-13 5/9/1995 2.21E-16 9.00E-14 2.25E-14 S.56E-16 2.00E-14 S.OOE-15 3.06E-15 9.00E-13 2.25E-13 4.34E-15 6.00E-13 150E-13 8/9/1995 1.66E-16 9.00E-14 2.25E-14 1.67E-15 2.00E-14 S.OOE-15 3.90E-15 9.00E-13 2,25E-13 5,60E-15 6.00E-13 1.50E-13 11/11/1995 2.04E-14 9.00E-14 2.25E-14 6.70E-15 2.00E-14 S.OOE-15 7.65E-15 9.00E-13 2,25E-13 4.47E-15 6.00E-13 1.50E-13 U5/1996 4.50E-14 9.00E-14 2.25E-14 3.58E-14 2.00E-14 S.OOE-15 2,39E-14 9.00E-13 2.25E-13 7.30E-15 6.00E-13 1,50E-13 5/6/1996 1.76E-15 9.00E-14 2.25E-14 3.57E-15 2"00E-14 S.OOE-15 9.55E-16 9.00E-13 2.25E-13 7,54E-15 G.OOE-13 1.50E-13 8/5/1996 2.37E-15 9.00E-14 2.25E-14 8,18E-15 2.00E-14 S.OOE-15 7.46E-16 9.00E-13 2.25E-13 5.75E-15 6.00E-13 1.50E-13 11/6/1996 3.53E-15 9.00E-14 2.25E-14 6.31E-15 2.00E-14 S.OOE-15 9.39E-16 9.00E-13 2.25E-13 1.21E-14 6.00E-13 L50E-13 2/6/1997 1.84E-16 9.00E-14 2.25E-14 2.01E-16 2.00E-14 S.OOE-15 1.87E-16 9.00E-13 2.25E-13 6.14E-15 6.00E-13 l.50E-13 5/5/1997 5.75E-16 9.00E-14 2.25E-14 7.24E-16 2.00E-14 S.OOE-15 6.07E-16 9.00E-13 2.25E-13 4.75E-15 6.00E-13 1.50E-13 8/11/1997 1.21E-15 9.00E-14 2.25E-14 7.39E-16 2.00E-14 S.OOE-15 5.05E-16 9.00E-13 2.25E-13 4.92E-15 G.OOE-13 l.SOE-13 1/5/1998 9.89E-16 9.00E-14 2.25E-14 1.92E-15 2.00E-14 S.OOE-15 6,21E-16 9.00E-13 2.25E-13 4.68E·15 6.00E-13 1.50E-13 4/28/1998 2,84E-15 9.00E-14 2.25E-14 2.38E-15 Z.OOE-14 5.00E-15 1.72E-15 9.00E-13 2.25E-13 7.35E·l5 6.00E-13 1.50E-13 7/31/1998 7.49E·l6 9.00E-14 2.25E-14 1.49E-15 2.00E-14 S.OOE-15 8.34E-16 9.00E-13 2.25E-13 7.01E-15 6.00E-13 1.50E-13 9/28/1998 1.07E-15 9.00E-14 2.25E·14 9.20E-16 2.00E-14 S.OOE-15 6.32E-16 9.00E-13 2.25E-13 3.95E-15 6.00E-13 1.50E-13 12/28/1998 8.51E-15 9.00E-14 2.25E-14 4.58E-15 2.00E-14 S,OOE-15 4.58E-15 9.00E-13 2.25E-13 1.43E-14 6.00E-13 1.50E-13 8/29/1999 3.75E-15 9.00E-14 2.25E-14 2.45E-15 Z.OOE-14 S,OOE-15 2.39E-15 9.00E-13 2.25E-13 8.46E-15 G.OOE-13 1.50E-13 7/3/1999 1.53E-15 9.00E-14 2.25E-14 8.65E-16 2.00E-14 S,OOE-15 6.52E-16 '9.00E-13 2.25E-13 7.20E-15 6.00E-13 1.50E-13 9/27/1999 5.83E-15 9.00E-14 2.25E-14 3.52E-15 2.00E-14 .S.OOE-15 2.55E-15 9.00E-13 2.25E-13 8.22E-15 6.00E-13 1.50E-13 12/28/1999 9.48E-15 9.00E-14 2.25E-14 6.20E-15 2.00E-14 S.OOE-15 3.96E-15 9,00E-13 2.25E-13 7.56E-15 6.00E-13 1.50E-13 3/27/2000 2.06E-15 9.00E-14 2.25E-14 1.27E-15 2.00E-14 S.OOE-15 1.09E-15 9~00E-13 2.25E-13 7.72E-15 6.00E-13 1.50E-13 6/26/2000 1.SOE-15 9.00E-14 2.25E-14 1.24E-15 2.00E-14 S,OOE-15 1.01E-15 9.00E-13 2.25E-13 4.36E-15 6~00E-13 1.50E-13 'J/26/2000 1.04E-15 9.00E-14 2.25E-14 5.45E-16 2.00E-14 S.OOE-15 6.01E-16 9.00E-13 2.25E-13 7.67E-15 6.00E-13 1.50E-13 12/26/2000 1.48E-15 9.00E-14 2.25E-14 7.56E-16 2.00E-14 S.OOE-15 6.84E-16 9,00E-13 2.25E-13 7.00E-15 6.00E-13 1.50E-13 3/26/2001 4.27E-16 9.00E-14 2.25E-14 2.19E-16 2.00E-14 S.OOE-15 1.89E-16 9.00E-13 2.25E-13 6.13E-15 G.OOE-13 1.50E-13 7/2/2001 4.52E-16 9.00E-14 2.25E-14 4,02E-16 2.00E-14 S.OOE-15 LOOE-16 9.DOE-13 2.25E-13 7.48E·15 G.OOE-13 1.50E-13 9/24/2001 4.65E-16 9.00E-14 2.25E-14 2.06E-16 2.00E-14 S.OOE-15 2.02E-16 9.00E-13 2.25E-13 6.98E-15 6.00E-13 1.SOE-13 12/31/2001 7.40E-16 9.00E-14 2.25E-14 3.51E-16 2.00E-14 S.OOE-15 3.64E-16 9.00E-13 2.25E-13 4.72E-15 6.00E-13 1.50E-13 4/1/2002 L26E-15 9.00E-14 2.25E-14 7.53E-16 2.00E-14 S.OOE-15 7.19E-16 g.OOE-13 2.25E-13 ~.65E-15 6.00E-13 1.50E-13 7/1/2002 1.02E-15 9.00E-14 2.25E-14 1.03E-15 2.00E-14 !i.OOE-15 3.39E-16 9.00E-13 2.25E-13 7.20E-15 6.00E-13 1.50E-13 9/30/2002 ;;.82E-16 9.00E-14 2.25E-14 9.28E-16 2.00E-14 :S.OOE-15 a.14E-16 '9.00E-13 2.25E-13 4.48E-15 6.00E-13 1.50E-13 12/30/2002 l.OOE-16 9.00E-14 2.25E-14 7.67E-16 2.00E-14 S,OOE-15 3.48E-16 fl.OOE-13 2.25E-13 9.56E-15 IJ.OOE-13 1.50E-13 3/31/2003 1.13E-15 9.00E-14 2.25E-14 7.41E-16 2.00E-14 S.OOE-15 4.41E-16 9.00E-13 2.25E-13 6.68E-15 p.OOE-13 1.50E-13 6/30/2003 4.35E-16 9.00E-14 2.25E-14 5.08E-16 2.00E-14 S.OOE-15 2.51E-16 S.OOE-13 2.25E-13 1.34E-15 6.00E-13 1.50E-13 9/29/2003 1.51E-16 9.00E-14 2.25E-14 1.02E-16 2.00E-14 !;,OOE-15 l.OOE-16 IJ.OOE-13 2.25E-13 7.28E-15 p.OOE-13 1.50E-13 12/29/2003 1.52E-16 9.00E-14 2.25E-14 1.54E-16 2.00E-14 S.OOE-15 1.51E-16 il.OOE-13 2.25E-13 7.02E-15 6.00E-13 1.50E-13 3/29/2004 1.00E-16 9.00E-14 2.25E-14 1.12E-16 2.00E-14 !>.OOE-15 l.OOE-16 IJ.OOE-13 2.25E-13 8.82E-15 p,OOE-13 1.SOE-13 6/27/2004 1.18E-16 ·9.00E-14 2.25E-14 3.11E-16 2.00E-14 5.00E-15 1.25E-16 9.00E-13 2.25E-13 2.47E-15 G.OOE-13 l.SOE-13 9/27/2004 1.16E-16 9.00E-14 2.25E-14 1.72E-16 2.00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 l.lOE-14 IJ.OOE-13 l.SOE-13 12/27/2004 1.14E-16 9.00E-14 2.25E-14 l.OGE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.59E·14 6.00E-13 1.SOE-13 3/28}2005 l.OOE-16 9.00E-14 2.25E-14 2.04E-16 2.00E-14 6.00E-15 1.83E-16 9.00E-13 2.25E-13 8.57E-15 G.OOE-13 1.50E-13 6/29/2005 1.83E-16 9.00E-14 2.25E-14 3.81E-16 2.00E-14 S.OOE-15 3.09E-16 9.00E-13 ,2.25E-13 1.06E-14 G.OOE-13 1.50E-13 9/26/2005 2.87E-16 9.00E-14 2.25E-14 8.21E-16 2,00E-14 5.00E-15 3.71E-14 9.00E-13 2.25E-13 6.28E-14 6.00E-13 1.50E-13 1/3/2006 8.74E-16 9.00E-14 2.25E-14 3.79E-16 2.00E-14 5.00E-15 1.31E-16 !:J.OOE-13 2.25E-13 4.32E-14 ~.OOE-13 1.50E-13 4/3/2006 5.22E-16 9.00E-14 2,25E-14 6.66E-16 2.00E-14 5.00E-15 1.11E-16 9.00E-13 1.25E-13 9.34E-15 6.00E-13 1.50E-13 7/3/2006 3.08E-16 9.00E-14 2.25E-14 1.10E-16 2.00E-14 5.00E-15 l.OOE-16 !l.OOE-13 2.25E-13 1.25E-14 6.00E-13 1.50E-13 10/2/2006 9.14E-16 9.00E-14 2.25E-14 4.95E-16 2.00E-14 5.00E-15 1.86E-16 9.00E-13 2.25E-13 L67E-14 6.00E-13 1.50E-13 1/1/2007 9.49E-16 9.00E-14 2.25E-14 6.81E-16 2.00E-14 5.00E-15 2.02E-16 l.l.OOE-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13 4/2/2007 1.08E-15 9.00E-14 2.25E-14 8.22E-16 2.00E-14 5.00E-15 2.26E-16 9.00E-13 2.25E-13 1.64E-14 6.00E-13 1,50E-13 7/2/2007 1.54E·15 B.OOE-14 2.25E-14 8.16E-16 2.00E-14 S.OOE-15 4.76E-16 9.00E-13 2.15E-13 2.12E·14 6.00E-13 1.50E-13 9/30/2007 4.90E-16 9.00E-14 2.25E-14 2.37E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 .Z.lSE-13 6.65E-15 6.00E-13 1.50E-13 12/31/2007 1.46E-15 B.OOE-14 2.2SE-14 5.67E-16 2.00E-14 S.OOE-15 l.OOE-16 9,00E-13 2.15E-13 1.02E-14 6 OOE-13 1.50E-13 3/31/2008 3.16E-16 9.00E-14 2.25E-14 6,17E-16 2,00E-14 5.00E-15 3.71E-16 9.00E-13 2.25E-13 4.82E-15 ~.OOE-13 1.50E-13 6/30/2008 3.13E-15 9.00E-14 2.25E-14 1.55E-15 2.00E-14 5.00E-15 9.27E-16 9,00E-13 2.25E-13 7.40E-15 fi.OOE-13 1.SOE-13 ----- Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml l!HV-ST Effluent Concentration Limit= 9E-13 uCi/ml BHV-SR Effluent Concentration Limit = 6E-13 uCi/ml :sHV-SPB ALARAGoal = 2.25E-14 uCi/ml ALARA Goal-SE-13 uCi/ml ALARAGoal = 2.25E-13 uCifml ALARA Goal-1.5E-13 uCi/ml Pre 1994 MPC Limit-SE-12 uCI/ml Pre 1994 MPC Limit= SE-14 uCi/ml Pre 1994 MPC Limit= 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL-1.25E-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 7.08E-15 9.00E-14 2.25E-14 3.41E-15 2 OOE-14 S.OOE-15 2.52E-15 9.00E-13 2.25E-13 1.15E-14 6.00E-13 l.SOE-13 12/31/2008 7.22E-15 9.00E-14 2.25E-14 2.82E-15 2.00E-14 6.00E-15 3.03E-15 9.00E-13 2.25E-13 1.59E-14 6.00E-13 1.50E-13 3/15/2009 4.13E-15 9.00E-14 2.25E-14 l.39E-15 2.00E-14 S.OOE-15 1.41E-15 9.00E-13 2.25E-13 4.66E-15 6.00E-13 l.SOE-13 6/15/2009 2.31E-16 9,00E-14 2.25E-14 7.79E-16 2.00E-14 S.OOE-15 6.37E-16 B.OOE-13 2.25E-13 4.18E-15 6.00E-13 l.50E-13 9/15/2009 3.10E-15 9.00E-14 2.25E-14 9.20E-16 2.00E-14 S.OOE-15 6.36E-16 9.00E-13 2.25E-13 1.21E-14 6.00E-13 1.50E-13 12/15/2009 S.77E-15 9.00E-14 2.25E-14 3.13E-16 2.00E-14 6.00E-15 1.92E-16 S.OOE-13 2.25E-13 2.48E-15 6.00E-13 1.50E-13 3/31/2010 4.78E-15 9.00E-14 2.25E-14 3.73E-16 2.00E-14 5.00E-15 4.19E-16 9.00E-13 2.25E-13 1.30E-14 6.00E-13 1.50E-13 6/30/2010 4.35E-15 9.00E-14 2.25E-14 7.84E-16 2.00E-14 S.OOE-15 1.05E-15 9.00E-13 2.25E-13 4.40E-15 6.00E-13 1.50E-13 9/30/2010 d.57E-15 9.00E-14 2.25E-14 1.14E-15 2.00E-14 6.00E-15 7.97E-16 !l.OOE-13 2.25E-13 .3.78E-15 p.OOE-13 1.50E-13 12/31/2010 8.52E-15 9.00E-14 2,25E-14 1.45E-15 2.00E-14 S.OOE-15 1.29E-15 9.00E-13 2.25E-13 1.33E-14 6.00E-13 1.50E-13 4/4/2011 3.20E-15 B.OOE-14 2.25E-14 8.89E-16 2.00E-14 S.OOE-15 l.lOE-15 f.l.OOE-13 2.25E-13 1.48E-14 6.00E-13 1.50E-13 7/4/2011 6.98E-15 9.00E-14 2.25E-14 2.03E-15 2.00E-14 S.OOE-15 2.52E-15 9.00E-13 2.25E-13 l.OBE-14 6.00E-13 1.50E-13 10/3/2011 3.11E-15 9.00E-14 2.25E-14 1.14E-15 2.00E-14 5.00E-15 5.75E-16 9.00E-13 2.25E-13 1.41E-14 6.00E-13 1.50E-13 1/3/2012 4.44E-15 9.00E-14 2.25E-14 2.14E-15 2.00E-14 S.OOE-15 1.53E-15 9.00E-13 2.25E-13 2.05E-14 6.00E-13 1.50E-13 4/3/2012 S.52E-15 9.00E-14 2.25E-14 3,24E-15 2.00E-14 S.OOE-15 1.79E-15 9.00E-13 2.25E-13 1.55E-14 6.00E-13 1.50E-13 7/2/2012 5.87E-15 l:l.OOE-14 2.25E-14 3.06E-15 2.00E-14 S.OOE-15 1.21E-15 9.00E-13 2.25E-13 1.11E-14 6.00E-13 1.50E-13 10/1/2012 6.73E-15 9.00E-14 2.25E-14 2.59E-15 2.00E-14 S.OOE-15 2.43E-15 9.00E-13 2.25E-13 1.30E-14 6,00E-13 1.50E-13 12/31/2012 4.50E-15 f.l.OOE-14 2.25E-14 1.62E-15 2.00E-14 S.OOE-15 1.79E-15 9.00E-13 2.25E-13 1.74E-14 6,00E-13 1.50E-13 3/25/2013 6.66E-15 9.00E-14 2.25E-14 1.48E-15 2.00E-14 S.OOE-15 1.12E-15 9.00E-13 2.25E-13 l.SOE-14 6.00E-13 1.50E-13 7/2/2013 7.35E-15 B.OOE-14 2.25E-14 1.72E-15 2.00E-14 S.OOE-15 2.02E-15 9.00E-13 2.25E-13 6,67E-15 6.00E-13 1.50E-13 9/30/2013 2.78E-15 9.00E-14 2.25E-14 6.92E-16 2.00E-14 5.00E-15 3.29E-16 9.00E-13 2.25E-13 6.62E-15 6.00E-13 1.50E-13 12/30/2013 6.70E-15 9.00E-14 '2.25E-14 3,93E-16 2.00E-14 5.00E-15 2.53E-16 9.00E-13 2.25E-13 2.78E-14 6.00E-13 1.SOE-13 3/31/2014 4.74E-15 9.00E-14 2.25E-14 1.42E-15 2.00E-14 S.OOE-15 3.48E-15 9.00E-13 2.25E-13 1.50E-14 6.00E-13 1.50E-13 6/30/2014 8,18E-15 IJ.OOE-14 2.25E-14 1.34E-15 2.00E-14 5.00E-15 1.76E-15 9.00E-13 2.25E-13 1.42E-14 6.00E-13 1.50E-13 - 1/) c 0 ... 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I llJ 0 ~ ,.... 8~-das c::~-das ~~-des o~-das 6o-das so-das Lo-des go-d as so-das -vo-das 8o-das c::o-das ~o-des oo-das 66-das B6-das L6·das 95-das 95-das t6-das 86-das c::5-das ~5-das 05-das 6B-das gg-das La-das gg-das gg-das -vs-das 8B-das c::s-das ~g-das Sep-81 Sep-82 Sep-83 Sep-84 Sep-85 Sep-86 Sep-87 Sep-88 Sep-89 Sep-90 Sep-91 Sep-92 Sep-93 Sep-94 Sep-95 Sep-96 Sep-97 Sep-98 Sep-99 Sep-00 Sep-01 Sep-02 Sep-03 Sep-04 Sep-05 Sep-06 Sep-07 Sep-08 Sep-09 Sep-10 Sep-11 Sep-12 Sep-13 0 0 m I _. "-- . - . - - - - . - - - - _. 0 0 m I _. 0) - ~ I _. 0 0 m I _. 01 ..... ~ II' ~· ~ r-.. ~ ~ b::::::::: f¥ !"'== ~r-~ ~ p~ ~~ ~ 1 .. r-+- ~ ~ ~ .! ~ I ~ (Log Scale) _. 0 0 0 0 m m I I _. _. ~ w ~ ~· ~ ~ :I ~~ D - I .. ~ ~ :::: I ' ~~ .... , 4 _. _. 0 0 0 0 m m I I ...... ...... 1\:) "O l>m .,r ::t CD Jioo -_.::D C: (l)]>g (I) .. -""C)o :S:o o "'0 ~::::1 o 11 n r CD -· Ul :I 3 r;n ~ -· ..... Col ; (,)g. co C:::::J r;n ~c ..... 3 3 -""--· c: -0 II ::::::.: 1\) 3 m -I ..... "'" c: 0 ~ tD ::I: ~ (J1 ~ :::r 0 :::::!. c: 3 I 1\) w 0 (") 0 ::l (') CD ::l -a c;· ::l Ul -c: (") ~ - --:§ (.) :::::s -(/) c 0 '+' t! -c CLI (.) c 0 (.) co C\1 C\1 I E :::::s "C cu a: Lt) ::> ~ m Li.J 0 C! ,.... ,..,..., .... . N (') ,.... ,.... I I lJJ lJJ 0 0 C! C! ,.... IA~L~ += ~ .. ~ ~ ~~ ~ - kl;; ---4 llllr. ~ .4<:':: r..~ • .. ~ • ~ s ""r--. ~ F-~ • '<:!" L() ,.... ,.... I I lJJ lJJ 0 0 0 C! (a1eos oo1) ~ 1'4r--::::::.• ... --.. r-N ~ ·~ f+" ~ ~f-.. > > -I I ~ ....... ~~ CD ,.... I lJJ 0 C! ,.... - - - - - - . >Oj - 1-- - - ,..._ ,.... I lJJ 0 C! 8~-das G~-das ~~-des o~-das 6o-das so-das Lo-das go-das go-das vo-das 8o-das Go-das ~o-das oo-das 66-das 86-das L6-das 96-das 96-das v6-das 86-das G6-das ~6-das 06-das 6s-das ss-das Ls-das gg-das gs-das vs-das 8s-das Gs-das ~s-das -:§ 0 ::::J -rn c 0 ; ca ... -c G) u c 0 0 0 ,.. ~ "C ca j ~ ::I: m T"'" T"'" I w 0 0 fill I .. • .. ~ t r. I• ~ -..:: ·~ C\J C') T"'" T"'" I I w w 0 0 ~ ~ T"'" T"'" Ito::: A ·~ .. ... ... ~ ~ ~ «:; ~ ~ ~ .::::: i"' t ~ • = r. , ~ ~ ::::::: ;! :!:. r-~ ~ ~ • ~ I; ~ ;: ~ !" I-.A. r"" ~ "<t T"'" I w 0 0 (ale:>s 6o1) • .. LO (0 T"'" T"'" I I w w 0 0 0 ~ - . . . . I'- T"'" I w 0 ~ 8~-das c~-das ~ ~-das o~·das 6o-das so-das La-das go-d as go-d as vo-das 8o-das co-das ~a-d as oo-das 66-das 95-das L6-das 95-das 95-das v6·das 86-das <::6-das ~5-das 05-das 6s-das ss-das LS·das gg-das gg-das vs-das 8s-das <::s-das ~g-das TAB6 BHV-6 AIR SAMPLING GRAPHS AND DATA TABLE Date Ufluent Concentration Limit = 9E-14 uCi/ml BHV-6U Effluent Concentration Limit = ZE-14 uCi/ml ~HV-6T Effluent Concentration Limit= 9E-13 uCi/ml 1!HV-6R Effluent Concentration Limit = ~E-13 uCi/ml BHV-6PB ALARA Goal= Z.ZSE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal= 2.25E-13 uCi/ml ALARA Goal= l.SE-13 uCi/ml Prl! 1994 MPC Limit= 5E-1ZuCi/ml Pre 1994 MPC Limit = BE-14 uCi/ml Pte 1994 l'y1PC Limit " 2E-1Z uCi/ml Pre 1994 MPC Urnlt" 4E-1Z uCi/ml Pre 1994 A LARA GOAL= l.ZSE-12 uCi/ml Pre 1994 ALARA GOAL= 5E-13 uCi/ml Pre 1994 ALARA GOAL -1E-1Z uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC ~FCA Cone ~FC EFCA 9/28/1981 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 12/14/1981 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 .2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 3/29/1982 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 .2.00E-12 S.OOE-13 4 OOE-12 l.OOE-12 6/30/1982 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 .Z.OOE-12 5,00E-13 4.00E-12 1.00E-12 9/27/1982 S.OOE-12 1.25E-12 g.OOE-14 2.00E-14 l ,OOE-12 ·s.OOE-13 4.00E-12 1.00E-12 1/3/1983 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 4/4/1983 S.OOE-12 1.25E-12 S.OOE-14 2.00E-14 l.OOE-12 S.OOE-13 4.00E-12 1.00E-12 6/30/1983 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 :Z,OOE-12 5 OOE-13 4.00E-12 1,00E-12 10/3/1983 S.OOE-12 1.25E-12 s.OOE-14 2.00E-14 l.OOE-12 S.OOE-13 4.00E-12 1.00E-12 1/3/1984 S.OOE-12 1.25E-12 s.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 4/2/1984 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E·12 5.00E-13 4.00E-12 l.OOE-12 7/2/1984 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 LOOE-12 10/1/1984 S,OOE-12 1.25E-12 8.00E-14 2.00E·14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 1/2/1985 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4-00E-12 l.OOE-12 4/1/1985 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1,00E-12 7/1/1985 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 9/30/1985 S.OOE-12 USE-12 S.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 1/2/1986 '5.00E-12 1.25E-12 8.00E-14 2,00E-14 2.00E-12 5,00E-13 4.00E-12 l.OOE-12 4/1/1986 S.OOE-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 6/30/1986 S.OOE-12 1.2SE-12 8.00E·14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 10/27/1986 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 12/15}1986 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2,00E-12 5.00E-13 4.00E-12 1.00E-12 3/16/1987 S.OOE-12 1.2SE-12 . S.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 5/11/1987 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 9/9/1987 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE·12 11/2/1987 .S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 2/16/1988 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E·12 5/18/1988 o.OOE-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1 OOE-12 8/15/1988 :S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 11/14/1988 S.OOE-12 1.2SE-12 8.00E-14 2,00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 2/13/1989 S.OOE-12 1.25E-12 S.OOE-14 2,00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 5/15/1989 5.00E-12 1.25E-12 B.OOE-14 MOE-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 .8/14/1989 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 11/13/1989 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 2/12/1990 5.00E-12 1.25E-12 8.00E-14 2,00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 5/14/1990 5.00E-12 1.25E-12 8.00E-14 2.00E-14 MOE-12 S.OOE-13 4.00E-12 l.OOE-12 8/13/1990 5.00E-12 l.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 11/12/1990 5.00E-12 1.2SE-12 e.ooe-14 2.00E-14 2,00E-12 S.OOE-13 4.00E-12 l.OOE-12 2/11/1991 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 5/13/1991 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5,00E-13 4.00E-12 l.OOE-12 8/12/1991 5.00E-12 1.2SE-12 S.OOE-14 2.00E-14 2,00E-12 5.00E-13 4,00E-12 1.00E-12 11}11/1991 5.00E-12 1.25E-12 g.OOE-14 2.00E-14 2,00E-12 S.OOE-13 4.00E-12 l.OOE-12 2/10/1992 5,00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE·12 S/11/1992 5,00E-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE·12 8/10/1992 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE·12 11/9/1992 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/9/1993 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4,00E-12 l.OOE-12 5/10/1993 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/10/1993 S,OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5,00E-13 4.00E-12 1.00E-12 11/8/1993 S .. OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E·12 l.OOE-12 2/7/1994 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l,OOE-12 5/9/1994 S,OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 8/9/1994 S,OOE-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12 11/7/1994 S,OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12 ------ Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-6U Effluent Concentration Limit= :ZE-14 uCi/ml-BHV-6T Effluent Concentration Limit= 9E-13 uCi/ml BHV-6R Effluent Concentration Limit = 6E-13 uCi/ml BHV-6PB ALARAGoal = 2.25E-14 uCi}ml ALARA Goal= SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARAGoal = l.SE-13 uCi/ml P«! 1994 MPC limit " 5E-12 uCi/ml Pre 1994 MPC Omll "' BE-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml Pre 1994 ALARA GOAL = .1.25E-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL= 1E-12 uCi/ml Cone EFC .EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 5)9/1995 9.00E-14 2.25E-14 ,2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 8/9/1995 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2,25E-13 6.00E-13 1.50E-13 11/11/1995 9.00E-14 :2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 2/5/1996 i:J.OOE-14 .2.25E-14 .2.00E-14 5.00E-15 9.00E-13 2,25E-13 6.00E-13 1.50E-13 5/6/1996 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 &/5/1996 .i:J,OOE-14 .2.25E-14 .2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1,50E-13 11/6/1996 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2..25E-13 6,00E-13 1.50E-13 2/6/1997 9.00E-14 .2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 5/5/1997 9.00E-14 ,2.25E-14 .2.00E-14 5.00E-15 9,00E-13 2.25E-13 6.00E-13 1.50E-13 8/11/1997 9.00E-14 .2.25E-14 .2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 1/5/1998 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 4/28/1998 9.00E-14 :2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 7/31/1998 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2,25E-13 6.00E-13 1.50E-13 9/28/1998 9.00E-14 :2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 12/28/1998 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 3/29/1999 9.00E-14 .2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 7/3/1999 9,00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13 9/27/1999 3,03E-15 9.00E-14 .2.25E-14 1.37E-15 .2.00E-14 5,00E-15 8.72E-16 9.00E-13 2.25E-13 7.55E-15 6.00E-13 1.50E-13 12/28/1999 5.01E-15 9.00E-14 2.25E-14 2.89E-15 2.00E-14 5.00E-15 1.31E-15 9.00E-13 2.25E-13 8.10E-15 6.00E-13 1,50E-13 3)30/2000 7.46E-16 9.00E-14 :2.25E-14 5.25E-16 2.00E-14 5.00E-15 3.00E-16 9.00E-13 2.25E-13 7.83E-15 6.00E-13 1.50E-13 6/26/2000 5.40E-16 !J.OOE-14 .2.25E-14 3.53E-16 2.00E-14 5.00E-15 6.11E-16 9.00E-13 2.25E-13 4.83E-15 6.00E-13 1.50E-13 9/25/2000 3,75E-16 9.00E-14 :2.25E-14 2.23E-16 2.00E-14 5.00E-15 1.91E-16 9.00E-13 2.25E-13 6.41E-15 6.00E-13 1.50E-13 12/26/2000 5.21E-16 9.00E-14 2.25E-14 3.39E-16 l.OOE-14 5.00E-15 3.28E-17 9.00E-13 2.25E-13 8.57E-15 6.00E-13 1.50E-13 3/26/2001 1.42E-16 9.00E-14 ,2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1,00E-16 9.00E-13 2.25E-13 6.15E-15 6.00E-13 1.50E-13 7/2/2001 1.81E-16 9.00E-14 :2.25E-14 1.66E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.95E-15 6.00E-13 1.50E-13 9/24/2001 3.08E-16 9.00E-14 ,2.25E-14 1.01E-16 2.00E-14 5.00E-15 1.77E-16 9.00E-13 2.25E-13 8.59E-15 6.00E-13 1.50E-13 12/31/2001 3.31E-16 9.00E-14 .2.25E-14 1.25E-16 .2.00E-14 5.00E-15 1.09E-16 9.00E-13 2.25E-13 3.14E-15 6.00E-13 1.50E-13 4/1/2002 4.77E-16 !J.OOE-14 .2.25E-14 2.94E-16 .2.00E-14 5.00E-15 1.96E-16 9.00E-13 2.25E-13 8.61E-15 6.00E-13 1.50E-13 7/1/2002 3.68E-16 9.00E-14 2.25E-14 4.41E-16 .2.00E-14 5,00E-15 1.76E-16 9.00E-13 2.25E-13 8.20E-15 6.00E-13 1.50E-13 9/30/2002 3.67E-16 9.00E-14 ,2.25E-14 5.60E-16 2.00E-14 5.00E-15 1.80E-16 9.00E-13 2.25E-13 5.55E-15 6,00E-13 1.50E-13 12/30/2002 1.00E-16 9.00E-14 .2.25E-14 3.43E-16 2.00E-14 5.00E-15 1.67E-16 9.00E-13 2.25E-13 1.35E-14 6.00E-13 1.50E-13 3/31/2003 1.98E-16 9.00E-14 ,2.25E-14 1.68E-16 ,2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.77E-15 6.00E-13 1.50E-13 6/30/2003 1,18E-16 g,OOE-14 ,2.25E-14 1.15E-16 ,2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.92E-15 6,00E-13 1.50E-13 9/29/2003 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 ,2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.30E-15 6.00E-13 1.50E-13 12/29/2003 1,00E-16 !).OOE-14 .2.25E-14 1.36E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.66E-15 6.00E-13 1.50E-13 3/29/2004 l.OOE-16 9.00E-14 .2.25E-14 l.OOE-16 .2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.17E-15 G.OOE-13 1.50E-13 6/27/2004 l.OOE-16 9.00E-14 .2.25E-14 l.OOE-16 ,2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 3.55E-15 G.OOE-13 1.50E-13 9/27/2004 l.OOE-16 9.00E-14 2.25E-14 1.38E-16 :Z.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2,25E-13 1.22E-14 6.00E-13 1.50E-13 12/27/2004 1.05E-16 9.00E-14 .2.25E-14 1.72E-16 .2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.52E-14 6.00E-13 1.50E-13 3/28/2005 l.OOE-16 9.00E-14 ,2,25E-14 l.OOE-16 ,2.00E-14 5.00E-15 l.OOE-16 9,00E-13 2.25E-13 9.34E-15 6.00E-13 1.50E-13 6/29/2005 1.28E-16 9.00E-14 .2.25E-14 1.01E-16 ,2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 9.85E-15 6.00E-13 1.50E-13 9/26/2005 1.98E-16 9.00E-14 .2.25E-14 5.98E-16 ,2.00E-14 5.00E-15 3.55E-16 9.00E-13 2,25E-13 1.71E-14 6,00E-13 1.50E-13 1/3/2006 7.67E-16 9.00E-14 2.25E-14 2.88E-16 .2.00E-14 5.00E-15 3.60E-15 9.00E-13 2.25E-13 4.85E-14 6.00E-13 1.50E-13 4/3/2006 2.92E-16 9.00E-14 ;2.25E-14 2.00E-16 ,2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2,25E-13 1.11E-14 6.00E-13 1.50E-13 7/3/2006 3.25E-16 9.00E-14 "2.25E-14 U6E-16 :2.00E-14 5.00E-15 1.08E-16 9.00E-13 2,25E-13 l.lOE-14 6.00E-13 1.50E-13 10/2/2006 5 03E-16 9.00E-14 ,2.25E-14 1.49E-16 2.00E-14 5.00E-15 1.19E-16 9.00E-13 2.25E-13 2.13E-15 6.00E-13 1.50E-13 1/1/2007 8.31E-16 9.00E-14 .2.25E-14 2.49E-16 .2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.70E-14 6.00E-13 1.50E-13 4/2/2007 5.36E-16 9.00E-14 .2.25E-14 3.15E-16 ,2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.43E-14 6.00E-13 1.50E-13 7/2/2007 1.08E-15 9.00E-14 ,2.25E-14 2.18E-16 2.00E-14 5.00E-15 1.54E-16 9.00E-13 2.25E-13 2.04E-14 6.00E-13 1.50E-13 9/30/2007 3.92E-16 9.00E-14 ,2.25E-14 1.02E-16 .2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.38E-15 6.00E-13 1.50E-13 12/31/2007 2.92E-15 9.00E-14 .2,25E-14 1.55E-15 2.00E-14 5,00E-15 3,16E-16 9.00E-13 2.25E-13 9.19E-15 6.00E-13 1.50E-13 3)31/2008 4.34E-16 9.00E-14 2.25E-14 ~.51E-16 .2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.99E-15 6.00E-13 1,50E-13 6/3102008 1.88E-15 9.00E-14 ,2.25E-14 9.00E-16 2.00E-14 5.00E-15 4.04E-16 9.00E-13 2.25E-13 7.41E-15 6.00E-13 1.SOE-13 Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-6U Effluent Concentration Limit= 2E-14 uCi/ml BHV-6T Effluent Concentration Limit= 9E-13 uCi/ml BHV-6R Effluent Concentration Limit= 6E-13 uCi/ml BHV-6PB ALARAGoal = 2.25E-14 uCi/ml ,<I.LARAGoal = SE-13 uCi/ml ALARA Goal= 2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 5E-12 uCi{ml Pre 1994 MPC Limit = BE-14 uCi/ml ~re 1994 MPC Limit= 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi}ml Pre 1994 ALARA GOAL = l.ZSE-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 4.82E-15 ~.OOE-14 '~.25E-14 2.10E-15 2.00E-14 S.OOE-15 1.27E-15 9.00E-13 2.25E-13 l.OOE-14 6.00E-13 1.50E-13 12/31/2008 4.80E-15 9.00E-14 2.25E-14 1.70E-15 .2.00E-14 5.00E-15 1.25E-15 9.00E-13 2.25E-13 1.49E-14 6.00E-13 1.50E-13 3/15/2009 2.77E-15 9.00E-14 2.25E-14 1.01E-15 .2.00E-14 5.00E-15 7.82E-16 9.00E-13 2.25E-13 6.46E-15 6.00E-13 1.50E-13 6/15/2009 1.41E-16 9.00E-14 .2.25E-14 2.67E-16 .Z.OOE-14 5.00E-15 1.81E-16 9.00E·13 2.25E-13 5.76E-15 6.00E-13 1.50E-13 9/15/2009 4.87E-15 9.00E-14 2.25E-14 4.32E-16 2.00E-14 5,00E-15 2.23E-16 9.00E-13 2.25E-13 8.98E-15 6.00E-13 1.50E-13 12/15/2009 9.24E-15 9.00E-14 .2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.15E-16 9.00E-13 2.25E-13 6.44E-15 6.00E-13 1.50E-13 3/31/2010 9.63E-15 9.00E-14 2.25E-14 1.82E-16 2.00E-14 5.00E-15 2.06E-16 9.00E-13 2.25E-13 1.37E-14 6.00E-13 1.50E-13 6/30/2010 3.62E-15 9.00E-14 2.25E-14 3.94E-16 2.00E-14 5.00E-15 4.89E-16 9.00E-13 2.25E·13 4.30E-15 6.00E-13 1.50E-13 9/30/2010 5.42E-15 ~.OOE-14 2.25E-14 1.08E-15 2.00E-14 5.00E-15 5.68E-16 9.00E-13 2.25E-13 3.98E-15 6.00E-13 1.50E-13 12/31/2010 1.24E-14 9.00E-14 .2.25E-14 1.21E-15 2.00E-14 5.00E-15 l.OOE-15 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 4/4/2011 2.70E-15 9.00E-14 .2.25E-14 4.62E-16 2.00E-14 5.00E-15 6.51E-16 9.00E-13 2.25E-13 1.29E-14 6.00E-13 1.50E-13 7/4/2011 3.01E-15 9.00E-14 .2.25E-14 7.07E-16 2.00E-14 5.00E-15 5.75E-16 9.00E-13 2.25E-13 7.97E-15 6.00E-13 1.50E-13 10/3/2011 2.05E-15 9.00E-14 2.25E-14 6.12E-16 2.00E-14 5.00E-15 1.88E-16 9.00E-13 2.25E-13 9.93E-15 6.00E-13 1.50E-13 1/3/2012 3.14E-15 9.00E-14 ·2.25E-14 1.09E-15 2.00E-14 5.00E-15 7.65E-16 9.00E-13 2.25E-13 1.89E-14 6.00E-13 1.50E-13 4/3/2012 4.41E-15 9.00E-14 ,2.25E-14 1.82E-15 2.00E-14 5.00E-15 4.00E-16 9.00E-13 2.25E-13 l.SOE-14 6.00E-13 1.50E-13 7/2/2012 6.42E-15 9.00E-14 2.25E-14 2.25E-15 2.00E-14 5.00E-15 5.11E-16 9.00E-13 2.25E-13 9.54E-15 6.00E-13 1.50E-13 10/1/2012 6.63E-15 9.00E-14 2.25E-14 1.31E-15 2.00E-14 5.00E-15 1.22E-15 9.00E-13 2.25E-13 1.34E-14 6.00E-13 1,50E-13 12/31/2012 3.83E-15 ~.OOE-14 2.25E-14 1.18E-15 2.00E-14 5.00E-15 9.30E-16 9.00E-13 2.25E-13 1.60E-14 6.00E-13 1.50E-13 3/25/2013 4.52E-15 9.00E-14 2.25E-14 7.93E-16 2.00E-14 5.00E-15 4.91E-16 9.00E-13 2.25E-13 1.70E-14 6.00E-13 1.50E-13 7/2/2013 5.91E-15 9.00E-14 2.25E-14 6.74E-16 2.00E-14 5.00E-15 7.85E-16 9.00E-13 2.25E-13 5.18E-15 6.00E-13 1.50E-13 9/30/2013 2.68E-15 9.00E-14 2.25E-14 3.97E-16 2.00E-14 5.00E-15 1.04E-16 9.00E-13 2.25E-13 6.13E-15 6.00E-13 1.50E-13 12/30/2013 1.60E-14 9.00E-14 2.25E-14 2.48E-16 2.00E-14 . 5.00E-15 1.05E-16 9.00E-13 2.25E-13 2.67E-14 6.00E-13 1.50E-13 3/31/2014 8.92E-15 9.00E-14 .2.25E-14 7.68E-16 2.00E-14 5.00E-15 1.50E-15 9.00E-13 2.25E-13 1.61E-14 6.00E-13 1.50E-13 6/30/2014 8.29E-15 9.00E-14 2.25E-14 5.35E-16 2.00E-14 5.00E-15 6.72E-16 9.00E-13 2.25E-13 l.ZOE-14 6.00E-13 1.50E-13 9/28/1981 4/4/1983 10/1/1984 4/1/1986 + 9/9/1987 c ~ 2/13/1989 c 3 z8/13/1990 a c Pl2/1 0/1992 + 8/10/1993 -1 ~ g_ 2/7/1995 c 3 ~ 8/5/1996 0 +4/28/1998 :::D ~9/27/1999 c 3 ,\)3/26/2001 1\) 0> + 9/30/2002 [; 3/29/2004 ~ ~9/26/2005 4/2/2007 9/30/2008 3/31/2010 10/3/2011 3/25/2013 f!l ...... 00 - - . 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I» II ~ 0 -""' ..... ::;, 11 m c r-_. I 0 -• m ..... ::::::3 .!..~3 ;::;: N o -n c o:::: CJ) o 3 m :::.:-.!.. 3 (o) -c 0 ~ OJ ::I: ~ 0) r-CD D) 0. I N ....... 0 0 0 ::::J () CD ::::J -~-0 ::::J en -c 0 ~ ..:::: ATTACHMENT C BHV AIR SAMPLING LABORATORY RESULTS AND QAJQC EI\ERGY L '1• t ,,,;.I :_d.JI ' www.energylab.com ,.,_ En:ellwlclstw. IIU Helena, MT 877-472-G711 • Billings, MT 101·735-440 • Casper, WV 811·235·1515 Gillett&, WY 11&-188· 7175 • Rapid Ctty, SD 118-872·1225 • College Station, TX 881-BUD-2211 May 20, 2014 Energy Fuels Resources (USA) Inc 225 Union Blvd Ste 600 Lakewood, CO 80228-1826 Work Order: C14040336 Project Name: 1st Quarter Air 2014 ANALYTICAL SUMMARY REPORT Energy Laboratories, Inc. Casper WY received the following 6 samples for Energy Fuels Resources (USA) Inc on 4/9/2014 for analysis. LabiD Client Sample ID Collect Date Receive Date Matrix Test c 14040336-001 BHV-1 03/31 /14 00:00 04/09/14 Filter Composite of two or more samples Field Parameters Metals, Total Digestion, Total Metals RAD Alternate Unit Reporting Air Filters Lead 210 Radium 226 Thorium, Isotopic c 14040336-002 BHV-2 03/31/14 00:00 04/09/14 Filter Same As Above C14040336-003 BHV-4 03/31 /14 00:00 04/09/14 Filter Same As Above C14040336-004 BHV-5 03/31/14 00:00 04/09/14 Filter Same As Above c 14040336-005 BHV-6 03/31/14 00:00 04/09/14 Filter Same As Above c 14040336-006 Blank 03/31/14 00:00 04/09/14 Filter Same As Above The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601 , unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the OA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Appmved By' ~ z kh,__- Acling Branch Manager · Digitally signed by Steve Carlston Date: 2014.05.20 11:51:25 -06:00 Page 1 of22 ·~·~· ... ~--·-··-....... --...... ~ ..................... --,. Gilletta, WY 818-688-117! • Rapid City, SD 888-&72·1225 • Collage station, TX 181-610-2218 CLIENT: Energy Fuels Resources (USA) Inc Project: 1st Quarter Air 2014 Sample Delivery Group: C14040336 ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Report Date: 05/20/14 CASE NARRATIVE Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b-Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r-Energy Laboratories, Inc. -Rapid City, SO eli-cs -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify Ell's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 22 EI\ERGY f', :-II-1,•, 1 ';.o .. JII •o www.energylab.com Mlfyt/AI ,..,. Sit/c. llfl Helena, MT 871·412·0711 • Billings, MT 800-735·4489 • Casper, WY 881·235·0515 Gillette, WY 866·686-7175 • Rapid City, SD 118·672-1225 • Collage station, TX 888·690·2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: May 20, 2014 PROJECT: 1st Quarter Air 2014 SAMPLE ID: BHV-1 Quarter/Date Sampled Concentration Radio nuclide Air Volume J1CilmL C14040336-001 ""'u 1.07E-15 First Quarter 2014 23oTh 2.07E-16 Air Volume in mLs 226Ra 3.69E-16 1.36E+11 2IOPb 1.24E-14 +LLD's are from NRC Reg. Guide 4.14 Counting Precision J1CilmL N/A 3E-17 3E-17 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2 Yearfor Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDC J1CilmL N/A 1E-17 IE-17 9E-17 L.L.D.+ Effluent Cone.* %Effluent 11CilmL J1CilmL Concentration 1E-16 9E-14 1.19E+00 1E-16 3E-14 6.91E-01 1E-16 9E-13 4.11E-02 2E-15 6E-13 2.07E+00 Page 3 of 22 EN:RGY f .1\ t<-:-. >I '..)UII ~ www.energylab.com IMifl/alm.r.-Siia ,. Helena, MT 817-412-0111 • Billings, MT BOD-735-4489 • Casper, WY 888-235-0515 Gillette, W'f 8&6-&8&-7175 • Rapid City, SD 818-172-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 1st Quarter Air 2014 LabiD: c 14040336-001 Client Sample ID: BHV-1 Analyses Result Units TRACE METALS -IN AIR Uranium 1.6E-09 mgiL Uranium, Activity 1.1 E-15 uCilmL RADIONUCLIDES-IN AIR Lead 210 1.2E-14 uCilmL Lead 210 precision (±) 2.3E-16 uCilmL Lead 210 MDC 9.4E-17 uCilmL Radium 226 3.7E-16 uCilmL Radium 226 precision (±) 2.7E-17 uCilmL Radium 226 MDC 1.0E-17 uCilmL Thorium 230 2.1E-16 uCilmL Thorium 230 precision (±) 3.3E-17 uCilmL Thorium 230 MDC 1.2E-17 uCilmL RADIONUCLIDES -IN AIR -PER FILTER Lead 210 Lead 21 0 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Uranium, Activity FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL -Anaiyte reporting limit. QCL-Quality control limit. 1700 pCiiFiiter 31.1 pCi!Fiiter 12.8 pCiiFilter 50.4 pCiiFilter 3.7 pCiiFiiter 1.4 pCiiFilter 28.3 pCiiFilter 4.5 pCi/Filter 1.6 pCiiFilter 146 pCiiFilter 136421082 L MDC -Minimum detectable concentration Qualifiers MCL/ RL QCL 1.5E-10 1.0E-16 0.20 Report Date: 05/20/14 Collection Date: 03/31/14 Date Received: 04/09/14 Matrix: Filter Method Analysis Date I By SW6020 04118114 12:08 I elm SW6020 04118114 12:08 I elm E909.0 05106114 18:051 eli-cs E909.0 05106114 18:05 I eli-cs E909.0 05106114 18:05 I eli-cs E903.0 04123114 06:38 lime E903.0 04123114 06:381imc E903.0 04123114 06:38 lime E908.0 04123114 13:37 I dmf E908.0 04123114 13:37 I dmf E908.0 04123114 13:37 I dmf RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05/15114 17:58 I sec RADCALC 05/15114 17:58 I sec RADCALC 05/15/14 17:58 I sec RADCALC 05115/14 17:58 I sec RADCALC 05/15/1417:58 I sec RADCALC 05115/14 17:58 I sec RADCALC 05/15114 17:58 I sec FIELD 03/31114 00:00 I*** MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of22 www.energylab.com INIIflai~SIIa 111n Helena, MT 177-472-0711 • BillinRs, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-616-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: May 20, 2014 PROJECT: 1st Quarter Air 2014 SAMPLE ID: BHV-2 Quarter/Date Sampled Concentration Radionuclide Air Volume ~CilmL C14040336-002 ""'U 4.63E-16 First Quarter 2014 23oTh 4.97E-17 Air Volume in mLs 226Ra 1.15E-16 1.36E+11 210Pb 1.49E-14 +LLD's are from NRC Reg. Guide 4.14 Counting Precision ~CilmL N/A 1E-17 9E-18 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDC~Ci/mL N/A 6E-18 3E-18 9E-17 L.L.D.+ Effluent Cone.* o/o Effluent ~Ci/mL ~CilmL Concentration 1E-16 9E-14 5.15E-01 1E-16 3E-14 1.66E-01 IE-16 9E-13 1.28E-02 2E-15 6E-13 2.48E+00 Page 5 of22 www.energylab.com EN:RGY I #\1 I ( )I • I'• I (_,;,t• ', MMtbl En:ellwa Slll:l 11!1 Helena, MT 817-412-11111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY IB&-&8&-7175 • Rapid City, SD 818-872-1225 • Collage Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 1st Quarter Air 2014 LabiD: c 14040336-002 Client Sample ID: BHV-2 Analyses Result Units TRACE METALS • IN AIR Uranium 6.8E-10 mgiL Uranium, Activity 4.6E-16 uCilmL RADIONUCLIDES • IN AIR Lead 210 1.5E-14 uCilmL Lead 21 0 precision (±) 2.4E-16 uCilmL Lead 210 MDC 9.1E-17 uCilmL Radium 226 1.2E-16 uCilmL Radium 226 precision (±) 8.6E-18 uCilmL Radium 226 MDC 3.2E-18 uCilmL Thorium 230 5.0E-17 uCilmL Thorium 230 precision (±) 1.0E-17 uCilmL Thorium 230 MDC 5.6E-18 uCi/mL RADIONUCLIDES • IN AIR -PER FILTER Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Uranium, Activity FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. 2030 pCi/Filter 33.4 pCiiFilter 12.4 pCiiFilter 15.7 pCiiFilter 1.2 pCiiFilter 0.44 pCiiFilter 6.8 pCiiFilter 1.4 pCiiFilter 0.76 pCiiFilter 63.2 pCiiFilter 136430085 L MDC -Minimum detectable concentration Qualifiers MCL! RL QCL 1.5E-10 1.0E-16 0.20 Report Date: 05/20/14 Collection Date: 03/31/14 DateReceived: 04/09/14 Matrix: Filter Method Analysis Date I By SW6020 0411811412:11 I elm SW6020 04118114 12:11 I elm E909.0 05106114 22:40 I eli-cs E909.0 05106114 22:40 I eli-cs E909.0 05106114 22:40 I eli-cs E903.0 04123114 06:38 I lmc E903.0 04123114 06:38 I lmc E903.0 04123114 06:38 I lmc E908.0 04123114 13:37 I dmt E908.0 04123114 13:37 I dmt E908.0 04123114 13:37 I dmt RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec FIELD 03131114 00:00 I*** MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 6 of 22 EI\ERGY ,~ I '' '' ~ ·, Jo J, I www.energylab.com IM/yl/al £JI:IIItlcl ~ IIJZ Helene, MT 877-472-0711 • Billings, MT BOD· 735-4489 • Casper, WY 888-235-0515 Gillette, WYB&&-&8&-7175 • Rapid City, SD 888-&72-1225 • College Station,lX 888-&90-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: May 20,2014 PROJECT: 1st Quarter Air 2014 SAMPLE ID: BHV -4 Quarterillate Sampled Concentration Radionuclide Air Volume J!CilmL C14040336-003 "''U 4.69E-15 First Quarter 2014 230Th 1.37E-16 Air Volume in mLs 226Ra 3.53E-16 1.35E+I I 210pb_ 1.08E-14 +LLD's are from NRC Reg. Guide 4.14 Counting Precision J!CilmL N/A 2E-17 2E-17 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCJJCilmL N/A 1E-17 SE-18 9E-17 L.L.D.+ Effluent Cone.* %Effluent JJCilmL J!CilmL Concentration 1E-16 9E-14 5.21E+00 1E-16 3E-14 4.58E-01 IE-16 9E-13 3.93E-02 2E-15 6E-13 1.81E+00 Page 7 of22 www.energylab.com EN:RGY I •'~•:lU I •J\l(_:IJ I _•_. IMiyllal Elcelltla Sllu II!Z Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillatts, WY 866-&86·7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 1st Quarter Air 2014 LabiD: c 14040336-003 Client Sample ID: BHV-4 Analyses Result Units TRACE METALS -IN AIR Uranium 6.9E-09 mgiL Uranium, Activity 4.7E-15 uCilmL RADIONUCLIDES • IN AIR Lead 210 1.1E-14 uCilmL Lead 210 precision (±) 2.1 E-16 uCilmL Lead 210 MDC 9.4E-17 uCilmL Radium 226 3.5E-16 uCilmL Radium 226 precision (±) 1.9E-17 uCilmL Radium 226 MDC 5.2E-18 uCilmL Thorium 230 1.4E-16 uCilmL Thorium 230 precision (±) 2.4E-17 uCilmL Thorium 230 MDC 1.0E-17 uCi/mL RADIONUCLIDES • IN AIR • PER FILTER Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Uranium, Activity FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. 1470 pCiiFilter 28.9 pCi/Filter 12.7 pCi/Filter 47.8 pCi/Filter 2.6 pCiiFilter 0.71 pCiiFilter 18.6 pCi/Filter 3.2 pCiiFilter 1.4 pCiiFilter 634 pCiiFilter 135285983 L MDC -Minimum detectable concentration Qualifiers MCL/ RL QCL 1.5E-1 0 1.0E-16 0.20 Report Date: 05/20/14 Collection Date: 03/31/14 Date Received: 04/09/14 Matrix: Filter Method Analysis Date I By SW6020 04118114 12:14 I elm SW6020 04118114 12:14 I elm E909.0 05107114 00:12 I eli-cs E909.0 05107114 00:12 I eli-cs E909.0 05107114 00:12 I eli-cs E903.0 04123114 06:38 I lmc E903.0 04123114 06:38 I lmc E903.0 04123114 06:38 I lmc E908.0 04123114 13:37 I dmf E908.0 04123114 13:37 I dmf E908.0 04123114 13:37 I dmf RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec FIELD 03131114 00:00 I ••• MCL -Maximum contaminant level. ND-Not detected at the reporting limit. Page 8 of22 www.energylab.com ANI1flal ~stm:e 1m Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 GilleHe, WY 866·686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: May 20,2014 PROJECT: 1st Quarter Air 2014 SAMPLE ID: BHV-5 Quarter/Date Sampled Concentration Radio nuclide Air Volume f.ICilmL C14040336-004 nalu 4.74E-15 First Quarter 2014 230Th 1.42E-15 Air Volume in mLs 226Ra 3.48E-15 1.35E+ll 210Pb l.SOE-14 +LLD's are from NRC Reg. Guide 4.14 Counting Precision f.ICilmL N/A IE-16 8E-17 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCf.ICilmL N/A 2E-17 IE-17 9E-17 L.L.D.+ Effluent Cone.* %Effluent f.ICilmL f.ICilmL Concentration IE-16 9E-14 5.27E+00 IE-16 3E-14 4.73E+00 IE-16 9E-13 3.86E-Ol 2E-15 6E-13 2.51E+00 Page 9 of22 www.energylab.com EI\ERGY l •• -,1_11 c. i l.:OI t il ~ Au11tJa1 EmiMct S.C. IIBI Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 888-686-7175 • Rapid City, SD 888-672-1225 • Collage Station, 1X 888-&90-221 8 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 1st Quarter Air 2014 Lab ID: c 14040336-004 Client Sample ID: BHV-5 Analyses Result Units TRACE METALS -IN AIR Uranium 7.0E-09 mgl l Uranium, Activity 4.7E-15 uCilml RADIONUCLIDES-IN AIR Lead 210 1.5E-14 uCilmL Lead 21 0 precision (±) 2.5E-16 uCilmL Lead 210 MDC 9.3E-17 uCilmL Radium 226 3.5E-15 uCilmL Radium 226 precision (±) 8.2E-17 uCilml Radium 226 MDC 1.0E-17 uCi/mL Thorium 230 1.4E-15 uCi/mL Thorium 230 precision (±) 1.5E-16 uCilmL Thorium 230 MDC 2.4E-17 uCilmL RADIONUCLIDES-IN AIR • PER FILTER Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Uranium, Activity FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. 2040 pCiiFilter 33.6 pCi/Filter 12.6 pCi/Filter 470 pCi/Filter 11 .1 pCiiFilter 1.4 pCi/Filter 192 pCi/Filter 20.1 pCiiFilter 3.2 pCiiFilter 641 pCiiFilter 135287479 L MDC -Minimum detectable concentration Qualifiers MCL/ RL OCL 1.5E-10 1.0E-16 0.20 Report Date: 05/20/14 Collection Date: 03/31/14 Date Received: 04/09/1 4 Matrix: Filter Method Analysis Date I By SW6020 0411811412:17 I elm SW6020 04118114 12:17 I elm E909.0 05107114 01 :43 I eli-cs E909.0 05/07114 01:43 I eli-cs E909.0 05/07114 01:43 I eli-cs E903.0 04123114 06:38 I lmc E903.0 04123114 06:38 I lmc E903.0 04123114 06:38 /lmc E908.0 04123/14 13:37 I dmf E908.0 04123114 13:37 I dmf E908.0 04123114 13:37 I dmf RADCALC 05115114 17:58 I sec RADCALC 05115/14 17:58 I sec RADCALC 05115/14 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05/15114 17:58 I sec RADCALC 05/15114 17:58 I sec RADCALC 05/15/14 17:58 I sec RADCALC 05/15114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec FIELD 03131114 00:00 I*** MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 22 EI\ERGY ! I • I ( • ~ .~ I t 'I <It 1 www.energylab.com Alllllf/UI EmiiMce Sltlct II$% Helena, MT 877-472-0711 • Billings, MT BOD-735·4489 • Casper, WY 188-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: May 20,2014 PROJECT: 1st Quarter Air 2014 SAMPLE ID: BHV-6 Quarter/Date Sampled Concentration Radionuclide Air Volume JJCilmL C14040336-005 ""U 8.92E-15 First Quarter 2014 23oTh 7.68E-16 Air Volume in mLs 226Ra l.SOE-15 1.35E+ll zwPb 1.61E-14 +LLD's are from NRC Reg. Guide 4.14 Counting Precision ,..cilmL N/A lE-16 4E-17 3E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCJ!CilmL N/A 2E-17 6E-18 9E-17 L.L.D.+ Effluent Cone.* %Effluent J.!CilmL J!CilmL Concentration lE-16 9E-14 9.91E+00 lE-16 3E-14 2.56E+00 IE-16 9E-13 1.67E-OI 2E-15 6E-13 2.69E+00 Page 11 of 22 EN:RGY t .-,-l ..... , ._11 ... 1• .: www.energytab.com AM/fbi~SIIu 1/I!Z Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 818-686-7175 • Rapid City, SD 118-672-1225 • College Station, 1X 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 1st Quarter Air 2014 LabiD: c 14040336-005 Client Sample ID: BHV-6 Analyses Result Units TRACE METALS-IN AIR Uranium 1.3E-08 mgiL Uranium, Activity 8.9E-15 uCilmL RADIONUCLIDES -IN AIR Lead 210 1.6E-14 uCilmL Lead 21 0 precision (±) 2.6E-16 uCi/mL Lead 210 MDC 9.2E-17 uCil mL Radium 226 1.5E-15 uCil mL Radium 226 precision (±) 4.0E-17 uCil mL Radium 226 MDC 5.7E-18 uCil mL Thorium 230 7.7E-16 uCi/mL Thorium 230 precision (±) 9.7E-17 uCilmL Thorium 230 MDC 1.7E-17 uCilmL RADIONUCLIDES-IN AIR-PER Fll TER Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Uranium, Activity FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. 2180 pCiiFilter 34.6 pCiiFilter 12.5 pCiiFilter 203 pCiiFilter 5.5 pCiiFilter 0.77 pCiiFilter 104 pCiiFilter 13.1 pCiiFilter 2.3 pCii Filter 1210 pCiiFilter 135283468 L MDC -Minimum detectable concentration Qualifiers MCL/ RL OCL 1.5E-10 1.0E-16 0.20 Report Date: 05/20/14 Collection Date: 03/31 /14 DateReceived: 04/09/14 Matrix: Filter Method Analysis Date I By SW6020 04118114 12:23 I elm SW6020 04118114 12:23 1 elm E909.0 05107114 03:151 eli-cs E909.0 05107114 03:151 eli-cs E909.0 05107114 03:15 I eli-cs E903.0 04123114 06:38 I lmc E903.0 04123114 06:38 l ime E903.0 04123114 06:38 l ime E908.0 04123114 13:37 I dmf E908.0 04123114 13:37 1 dmf E908.0 04123114 13:37 I dmf RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 0511511417:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec FIELD 03131114 00:00 I*** MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 12 of22 www.energylab.com A/llfrt/UI ~S/Jtef IISI Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO BBB-612-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: May 20,2014 PROJECT: 1st Quarter Air 2014 SAMPLE ID: Blank Quarter/Date Sampled Concentration Radionuclide Air Volume J!CilmL C14040336-006 natu 1.46E-17 First Quarter 2014 230Th 1.98E-18 Air Volume in mLs 226Ra 2.79E-18 1.36E+II 210Pb -1.20E-17 Counting Precision J!CilmL N/A lE-18 2E-18 4E-17 Note: Th1s sample uses 136,000,000 L of air volume for companson purposes. +LLD's are from NRC Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21 0 MDC J!CilmL N/A 2E-18 2E-18 7E-17 L.L.D.+ Effluent Cone.* %Effluent J!Ci/mL J!CilmL Concentration 1E-16 9E-14 1.62E-02 1E-16 3E-14 6.60E-03 IE-16 9E-13 3.10E-04 2E-15 6E-13 -2.0JE-03 Page 13 of22 EN:RGY I /\• I~,,-, l· 1 ' Ill! '.l www.energylab.com AMiybl E'Balleta Slllu 11152 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-8515 Gillette, WY 866-686-7115 • Rapid Crty, SD 888-612-1225 • College Station, TX 888-690-2218 LABORATORY ANAL VTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 1st Quarter Air 2014 Lab ID: c 14040336-006 Client Sample ID: Blank Analyses TRACE METALS -IN AIR Uranium Uranium, Activity RADIONUCLIDES -IN AIR Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC RADIONUCLIDES-IN AIR-PER FILTER Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Uranium, Activity FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. Result Units 0.0029 mgll 2.0E-09 uCilmL -1.6E-09 uCilmL 5.3E-09 uCilmL 9.0E-09 uCilmL 3.8E-10 uCilmL 2.2E-10 uCilmL 2.8E-10 uCilmL 2.7E-10 uCilmL 1.6E-10 uCilmL 2.1E-10 uCilmL -1.6 pCi!Filter 5.3 pCi/Filter 9.0 pCiiFilter 0.38 pCiiFilter 0.22 pCiiFilter 0.28 pCiiFilter 0.27 pCiiFilter 0.16 pCiiFilter 0.21 pCiiFilter 2.0 pCiiFilter 1 L MDC -Minimum detectable concentration Qualifiers D D u u U -Not detected at minimum detectable concentration MCL/ RL QCL 0.000043 2.9E-11 0.20 Report Date: 05/20/14 Collection Date: 03/31/14 Date Received: 04/09/14 Matrix: Filter Method Analysis Date I By SW6020 04118114 12:36 I elm SW6020 04118114 12:36 I elm E909.0 05107114 04:46 I eli-cs E909.0 05107114 04:46 I eli-cs E909.0 05107114 04:46 I eli-cs E903.0 04123114 06:38 I lmc E903.0 04123114 06:38 I lmc E903.0 04123114 06:38 I lmc E908.0 04123114 13:37 I dmf E908.0 04123114 13:37 I dmf E908.0 04123114 13:37 I dmf RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec RADCALC 05115114 17:58 I sec FIELD 03131114 00:00 I *** MCL -Maximum contaminant level. ND-Not detected at the reporting limit. D -RL increased due to sample matrix. Page 14 of22 EN:RGY l .~. ~ l 1• ) J. ~A· I _j( "I. -' www.energylab.com AM/yfii:M Eml/wJu SIRu ISU Helena, MT 811-412·0711 • Billings, MT 800-735·4489 • Casper, WV 888-235-1515 Gillatta, WY 8&&-&86-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-&90-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 1st Quarter Air 2014 Analyte Method: E903.0 Lab ID: C 14040336-004AD UP Radium 226 Radium 226 precision (±) Radium 226 MDC Lab ID: C14040336-005AMS Radium 226 Lab ID: LCS-41112 Radium 226 Lab ID: MB-41112 Radium 226 Radium 226 precision (±) Radium 226 MDC Qualifiers: RL -Analyte reporting limit. Count Result Units 3 Sample Duplicate 3.50E·06 pCi/L 8.30E-08 pCi/L 1.03E-08 pCi/L Sample Matrix Spike 2.82E-06 pCi/L Laboratory Control Sample 23.6 pCi/L 3 Method Blank ·0.05 pCi/L 0.1 pCi/L 0.2 pCi/L MDC · Minimum detectable concentration Report Date: 05/20/14 Work Order: C14040336 RL %REC Low Limit High Limit RPD RPDLimit Qual Run: BERTHOLD 770·2_140417A 0.5 Run: BERTHOLD 770·2_140417A 116 70 130 Run: BERTHOLD 770·2 140417A 110 80 120 Run: BERTHOLD 770·2_140417 A ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: 41112 04/23/14 06:38 14.7 04/23/14 06:38 04/23/14 06:38 04/23/14 09:43 u Page 15 of 22 EN:RGY l ·~~,,p,q tJI: ~ www.energylab.com Allll/ffiDM En:tlltwl&l Slla 1152 Helena, MT 817-472-0711 • Billings, MT 800-735·4489 • Casper, WV 888-235-1515 Gillatta, WV 8&&-&8&-7175 • Rapid City, SD 888-&72-1225 • College Station, 1X 888-690-!218 QAJQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 1st Quarter Air 2014 Analyte Count Result Units Method: E908.0 Lab ID: C14040336-002AMS Thorium 230 Lab ID: C14040336-002AMSD Thorium 230 Lab ID: LCS-41112 Thorium 230 Lab ID: MB-41112 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Qualifiers: RL -Analyte reporting limit. 3 MDC - Minimum detectable concentration Sample Matrix Spike 1.18E-06 pCi/L Sample Matrix Spike Duplicate 1.21 E-06 pCi/L Laboratory Control Sample 27.6 pCi/L Method Blank 0.4 pCi/L 0.2 pCi/L 0.3 pCi/L Report Date: 05/20/14 Work Order: C14040336 RL %REC Low Limit High Limit RPD RPDLimit Qual Run:ALPHANALYST_140421A 98 70 130 Run: ALPHANAL YST _140421 A 101 70 130 3.1 Run:ALPHANALYST_140421A 104 80 120 Run:ALPHANALYST_140421A NO -Not detected at the reporting limit. Batch: 41112 04/23/14 13:37 04/23/14 13:37 29.5 04/23/14 13:37 04/23/1413:37 Page 16 of 22 EI\ERGY l 1\ • It ! I ,• '• I 1_; I~· I· '-• www.energylab.com IM/fllai~S'-JJU Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY BBB-235-1515 Gillette, WY 866-686-7115 • Rapid City, Sll 888-672-1225 • College Station, TX 888-690-2218 QAJQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 1st Quarter Air 2014 Analyte Count Result Units Method: E909.0 Lab ID: LCS-21048 Lead 210 Lab ID: MB-21048 Lead 210 Lead 21 0 precision (±) Lead 210 MDC Lab ID: C14040336-001AMS Lead 210 Lab ID: C14040336-001AMSD Lead 210 Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration Laboratory Control Sample 103 pCi/L Method Blank -3 pCi/L 5 pCi/L 9 pCi/L Sample Matrix Spike 1.78E-05 pCi/L Sample Matrix Spike Duplicate 1.74E-05 pCi/L Report Date: 05/20/14 Work Order: C14040336 RL %REC Low Limit High Limit Run: SUB-T56720 81 80 120 Run: SUB-T56720 Run: SUB-T56720 125 70 130 Run: SUB-T56720 115 70 130 NO-Not detected at the reporting limit. RPD RPDLimit Qual 2.7 Batch: T~21 048 05/06/14 15:02 05/06/14 16:34 u 05/06/14 19:37 05/06/14 21 :08 15.8 U -Not detected at minimum detectable concentration Page 17 of 22 ·-El\ERGY www.energylab.com Helena, MT 877-472-011 t • Billings, MT 801·735-4489 • Casper, WY 888-235·1515 Gillatts, WY 866-68&-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690·2218 I 1\ • ~ l I ·.,I · .!i 'I· • AM/ftk:M Etwlltlta Sl1lr:l IIIU QAJQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 1st Quarter Air 2014 I Analyte Count Result Method: SW6020 Units Report Date: 05/20/14 Work Order: C14040336 RL %REC Low Limit High Limit RPD RPDLimit Qual Lab ID: ICV Initial Calibration Verification Standard Analytical Run: ICPMS2-C_140417A 04/18/14 10:35 Uranium Lab ID: ICSA Uranium LabiD: ICSAB Uranium Method: SW6020 Lab 10: MB-41112 Uranium Lab ID: LCS2-41112 Uranium Lab 10: C14040336·004ADIL Uranium Lab 10: C14040336-006AMS Uranium LabiD: C14040336·006AMSD Uranium Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration 0.0499 mg/L 0.00030 100 90 110 Interference Check Sample A 0.000634 mg/L 0.00030 Interference Check Sample AB -0.000259 mg/L 0.00030 Method Blank Run: ICPMS2-C_140417A ND mg/L 4E-05 Laboratory Control Sample Run: ICPMS2-C_140417A 0.0974 mg/L 4.3E-05 97 85 115 Serial Dilution Run : ICPMS2-C_140417A 6.38E-09 mg/L 1.5E-10 Sample Matrix Spike Run : ICPMS2-C_140417A 0.256 mg/L 4.3E-05 101 75 125 Sample Matrix Spike Duplicate Run: ICPMS2-C_140417A 0.262 mg/L 4.3E-05 104 75 125 ND -Not detected at the reporting limit. 9.3 2.3 04/18/14 10:38 04/18/14 10:41 Batch: 41112 04/18/14 11 :58 04/18/14 12:01 04/18/14 12:20 20 04/18/14 12:39 04/18/14 12:42 20 Page 18 of 22 EI\ERGY : 1\ !' r •· I' Jt-'1 www.energylab.com AMI1flal ElrfiiMa .. 1152 Helena, MT 877-472-0711 • Billings, MT 800-73!1-4489 • Casper, WY 888-235-0!115 Gillette, WY 866-686-7175 • Rapid City, SO 888-172-122!1 • College Station, TX 888-&90-2211 Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Corinne Wagner Reviewed by: Reviewed Date: BL2000\khelm 4/11/2014 Shipping container/cooler in good condition? Custody seals intact on all shipping container(s)/cooler(s)? Custody seals intact on all sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.) Temp Blank received in all shipping container(s)/cooler(s)? Container/Temp Blank temperature: Water-VOA vials have zero headspace? Water-pH acceptable upon receipt? Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes D N/A'C Yes D Yes D C14040336 Date Received: 4/9/2014 Received by: dcq NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD Carrier Next Day Air name: Not Present D Not Present D Not Present 0 Not Applicable 0 NoVOA vials submitted 0 Not Applicable 0 ---------------------------------------------------------------------------------~ Standard Reporting Procedures: Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Contact and Corrective Action Comments: None Page 19 of 22 Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: Energy Laboratories Contact: Garrin Palmer -=2:..;.;39.,;;.;3~Sf-a.:,;.lt;;;.;;C~r.;..;ee;;.;,.k~H,;.;;.wy-=--------Ph: 435 678 4115 Casper WY, 82601 gpalmer@energyfuels.com Chain of Custody/Sampling Analysis Request Project Samplers Name Samplers Signature 1st Quarter Air 2014 Garrin Palmer I Time SampleiD Date Collected Collected Laboratory Anal~sis Requested BHV-1 12/30/14-3/31/14 NA U-NAT, TH-230, Ra-226, Pb-210 BHV-2 12/30/14-3/31/14 NA U-NAT, TH-230, Ra-226, Pb-210 BHV-4 12/30/14-3/31114 NA U-NAT, TH-230, Ra-226, Pb-210 BHV-5 12130/14-3/31/14 NA U-NAT, TH-230, Ra-226, Pb-210 BHV-6 12/30/14-3/31/14 NA U-NAT. TH-230, Ra-226, Pb-21 0 Blank 12/30/14-3/31/14 NA U-NAT, TH-230, Ra-226, Pb-21 0 Comments: Relinquished By:(Signature) DateTTime Received By:(Signature) Datemme Garrin Palmer 4/7/2014 1230 ReliGI~ig~ Date/Time Received By:(Signature) DatefTime ~~~~ 4lq}14 q, ~I b www.energylab.com EI\ERGY I I' •• ' 'I~ I • , I! Alfll1l/rll blllltla lila 1111 Halana, MT 877-472-0711 • Billings, MT 800·738·4488 • Caspar, WY 888·235·8515 Gillette, WY 888-888-7171 • Rapid City, SD 111·872·1221 • Collage station, TX 888·81D-Z211 ANALYTICAL SUMMARY REPORT July 29, 2014 Energy Fuels Resources (USA) Inc 225 Union Blvd Ste 600 Lakewood, CO 80228-1826 Work Order: C 14070123 Project Name: 2nd Quarter Air 2014 Energy Laboratories, Inc. Casper WY received the following 6 samples for Energy Fuels Resources (USA) Inc on 7/2/2014 for analysis. LabiD Client Sample ID Collect Date Receive Date Matrix Test C14070123-001 BHV-1 06/30/14 00:00 07/02/14 Filter Composite of two or more samples Field Parameters Metals, Total Digestion, Total Metals RAD Alternate Unit Reporting Air Filters Lead 21 o Radium 226 Thorium, Isotopic c 14070123-002 BHV-2 06/30/14 00:00 07/02/14 Filter Same As Above c 14070123-003 BHV-4 06/30/14 00:00 07/02/14 Filter Same As Above c 14070123-004 BHV-5 06/30/14 00:00 07/02/14 Filter Same As Above C14070123-005 BHV-6 06/30/14 00:00 07/02/14 Filter Same As Above c 14070123-006 Blank 06/30/14 00:00 07/02/14 Filter Same As Above The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: Digitally signed by Steve Carlston Date: 2014.07.29 16:49:21 -06:00 Page 1 of 22 ........ -... , .......... -·--·--.......... -........ ...... ·-·--... ...-.. -· ....... .. Glllattl, WY 888-8811-7175 • Rapid City, SD 888-&72-1225 • Collage Station, IX 888-680-2218 CLIENT: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Air 2014 Sample Delivery Group: C14070123 ANALYTICAL COMMENTS Report Date: 07/29/14 CASE NARRATIVE Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4'C (±2'C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b-Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r-Energy Laboratories, Inc. -Rapid City, SO eli-cs -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: US EPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify Ell's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of22 www.energylab.com AnlfYIIul &ullwlu Slnr:. IIU Halana, MT 877-412-0711 • Billings, MT BDD-735-4481 • Casper, W'/888-235-0515 Gillette, WY B&B-&8&-7175 • Rapid City, SD 888-812-1225 • College Station, 1X 888·690·2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: July 29,2014 PROJECT: 2nd Quarter Air 2014 SAMPLEID: BHV-1 Quarterillate Sampled Concentration Air Volume Radionuclide JiCilmL C14040336-001 ""U 1.07E-15 First Quarter 2014 23uTh 2.07E-16 Air Volume in mLs 226Ra 3.69E-16 1.36E+l1 2\0J>b 1.24E-14 Quarterillate Sampled Concentration Radionuclide Air Volume 11CilmL C14070123-001 ""U 2.24E-15 Second Quarter 2014 230Th 5.14E-16 Air Volume in mLs 226Ra 1.09E-15 1.36E+11 210Pb 1.23E-14 +LLD's are from NRC Reg. Guide 4.14 Counting Precision JiCilmL N/A 3E-17 3E-17 2E-16 Counting Precision JiCi/mL N/A 6E-17 IE-17 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDC JiCilmL N/A 1E-17 1E-17 9E-17 MDC 11CilmL N/A 1E-17 2E-18 7E-17 L.L.D.+ Effluent Cone.* %Effluent 11CilmL JiCilmL Concentration lE-16 9E-14 1.19E+00 IE-16 3E-14 6.91E-Ol 1E-16 9E-13 4.11E-02 2E-15 6E-13 2.07E+00 L.L.D.+ Effluent Cone.* % Eftluent 11CilmL JiCilmL Concentration IE-16 9E-14 2.49E+00 lE-16 3E-14 1.71E+00 lE-16 9E-13 1.22E-01 2E-15 6E-13 2.06E+OO Page 3 of22 EN:RGY I l\ ~ , ~ I • ._ I • • f .Jit ~ www.energylab.com ~ Elr:tlllwa Slllclll!l Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-0515 Gillette, WY 118-681-7115 • Rapid City, SD 118-172-1225 • Collage Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Air 2014 Lab ID: c 14070123-001 Client Sample ID: BHV-1 Analyses Result Units TRACE METALS -IN AIR Uranium 3.3E-09 mgiL RADIONUCLIDES • IN AIR Lead 210 1.2E-14 uCi/mL Lead 21 0 precision (±) 2.0E-16 uCilmL Lead 210 MDC 7.0E-17 uCilmL Radium 226 1.1 E-15 uCilmL Radium 226 precision (±) 1.3E-17 uCilmL Radium 226 MDC 1.9E-18 uCilmL Thorium 230 5.1E-16 uCilmL Thorium 230 precision (±) 6.0E-17 uCi/mL Thorium 230 MDC 9.8E-18 uCilmL Uranium, Activity 2.2E-15 uCilmL RADIONUCLIDES · IN AIR-PER FILTER Lead 210 Lead 21 0 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Uranium, Activity FIELD PARAMETERS Air Filtering Volume *** Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. 1680 pCi/Filter 27.3 pCi!Filter 9.5 pCi!Filter 149 pCi/Filter 1.7 pCiiFilter 0.26 pCiiFilter 69.8 pCiiFilter 8.2 pCiiFilter 1.3 pCi/Filter 305 pCiiFilter 135988725 L MDC -Minimum detectable concentration Qualifiers MCL! RL QCL 1.5E-10 1.0E-16 0.20 Report Date: 07/29/14 Collection Date: 06/30/14 DateReceived: 07/02/14 Matrix: Filter Method Analysis Date I By SW6020 07110114 23:44 1 elm E909.0 07127114 04:241 eli-cs E909.0 07127114 04:241 eli-cs E909.0 07127114 04:241 eli-cs E903.0 07115114 19:131 dmf E903.0 07115114 19:131 dmf E903.0 07115114 19:13 1 dmf E908.0 07115114 09:06 I dmf E908.0 07115114 09:06 I dmf E908.0 07115114 09:06 I dmf SW6020 07/1 0/14 23:44 I elm RADCALC 07129/14 14:261 smm RADCALC 07/29/14 14:261 smm RADCALC 07/29/14 14:261 smm RADCALC 07/29/14 14:261 smm RADCALC 07/29/14 14:26 1 smm RADCALC 07129114 14:26 I smm RADCALC 07/2911414:26/ smm RADCALC 07/29114 14:26/ smm RADCALC 07/29114 14:26 / smm RADCALC 07/29114 14:26/ smm FIELD 06130/14 00:00 I *** MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 4 of 22 www.energylab.com Anl/1llal ~ SIIHIIIIIZ Helena, MT 871·412-0711 • Billings, 11fT 800·735·4481 • Casper, WY 888·235·0515 Gillette, WY 866·686-7175 • Rapid City, SD 888·612·1225 • College Station, TX 888-690·2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: July 29, 2014 PROJECT: 2nd Quarter Air 2014 SAMPLE ID: BHV-2 Quarter/Date Sampled Concentration Radionuclide Air Volume flCilmL C14040336-002 natu 4.63E-16 First Quarter 2014 23oTh 4.97E-17 Air Volume in mLs 226Ra 1.15E-16 1.36E+I1 2JUPb 1.49E-14 Quarter/Date Sampled Concentration Radionuclide Air Volume flCilmL c 14070123-002 oatu 3.04E-16 Second Quarter 2014 23oTh 7.92E-17 Air Volume in mLs 226Ra 1.82E-16 1.38E+ 11 210Ph 1.21E-14 +LLD's are from NRC Reg. Guide 4.14 Counting Precision flCilmL N/A 1E-17 9E-18 2E-16 Counting Precision flCilmL N/A 1E-17 5E-18 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21 0 MDC flCilmL N/A 6E-18 3E-18 9E-17 MDC flCilmL N/A 6E-18 2E-18 7E-17 L.L.D.+ Effluent Cone.* %Effluent flCi/mL flCilmL Concentration 1E-16 9E-14 5.15E-01 1E-16 3E-14 1.66E-01 1E-16 9E-13 1.28E-02 2E-15 6E-13 2.48E+00 L.L.D.+ Effluent Cone.* %Effluent flCilmL flCi/mL Concentration IE-16 9E-14 3.38E-OI 1E-16 3E-14 2.64E-01 1E-16 9E-13 2.02E-02 2E-15 6E-13 2.01E+00 Page 5 of22 E~RGY 1 1\•.L.!h I '..JHI. · www.energyleb.com Mllytlal br:llllluf ., 11!1 Helena, MT 877-472-0711 • Blllin1s. MT BGD-735-4419 • Caspar, WY 888-235-0515 Gillette, W/888-888-7115 • Rapid City, SD 818-872-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Air 2014 LabiD: c 14070123-002 Client Sample ID: BHV-2 Analyses Result Units TRACE METALS -IN AIR Uranium 4.5E-10 mgiL RADIONUCLIDES-IN AIR Lead 210 1.2E-14 uCilmL Lead 210 precision(±) 2.0E-16 uCilmL Lead 210 MDC 6.9E-17 uCilmL Radium 226 1.8E-16 uCilmL Radium 226 precision (±) 5.1E-18 uCilmL Radium 226 MDC 1.8E-18 uCilmL Thorium 230 7.9E-17 uCilmL Thorium 230 precision (±) 1.4E-17 uCilmL Thorium 230 MDC 5.7E-18 uCilmL Uranium, Activity 3.0E-16 uCilmL RADIONUCLIDES-IN AIR -PER FILTER Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Uranium, Activity FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. 1660 pCi/Filter 27.1 pCiiFilter 9.5 pCiiFilter 25.0 pCi!Filter 0.70 pCii Filter 0.25 pCiiFilter 10.9 pCiiFilter 1.9 pCiiFilter 0.79 pCiiFilter 41.8 pCiiFilter 137536199 L MDC -Minimum detectable concentration Qualifiers MCL/ RL QCL 1.5E-10 1.0E-16 0.20 Report Date: 07/29/14 Collection Date: 06/30/14 DateReceived: 07/02/14 Matrix: Filter Method Analysis Date I By SW6020 07110114 23:47 I elm E909.0 07127114 08:25 I eli-cs E909.0 07127114 08:25 I eli-cs E909.0 07127114 08:25 I eli-cs E903.0 0711511419:13ldmf E903.0 07115114 19:13 I dmf E903.0 07115114 19:13 I dmf E908.0 07115114 09:06 I dmf E908.0 07115114 09:06 / dmf E908.0 07/15/14 09:06 I dmf SW6020 07110114 23:47 I elm RADCALC 07129114 14:26 I smm RADCALC 07129/1414:26/ smm RADCALC 07129/1414:26/ smm RADCALC 07/29/14 14:26/ smm RADCALC 07/29/14 14:26 I smm RADCALC 07/29114 14:26 I smm RADCALC 07129114 14:26 I smm RADCALC 07129114 14:26 I smm RADCALC 07129114 14:26 I smm RADCALC 07129114 14:26 I smm FIELD 06130114 00:00 I*** MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of22 www.energylab.com Ataf1tlul&u"-$/Mt fW Helena, MT 877-412-0711 • Billinas, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-&72-1225 • Golleae Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: July 29,2014 PROJECT: 2nd Quarter Air 2014 SAMPLE ID: BHV-4 Quarter/Date Sampled Concentration Radionuclide Air Volume ,..cilmL c 14040336-003 nalu 4.69E-15 First Quarter 2014 23oTh 1.37E-16 Air Volume in mLs 226Ra 3.53E-16 1.35E+ll 210Eb 1.08E-14 Quarter/Date Sampled Concentration Radionuclide Air Volume flCi/mL C14070123-003 nalu 4.16E-15 Second Quarter 2014 23oTh 6.96E-16 Air Volume in mLs 226Ra 1.77E-15 1.37E+ll 210Ph 1.06E-14 +LLD's are from NRC Reg. Guide 4.14 Counting Precision flCi/mL N/A 2E-17 2E-17 2E-16 Counting Precision flCi/mL N/A 8E-17 2E-17 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDC flCi/mL N/A IE-17 SE-18 9E-17 MDC flCi/mL N/A 8E-18 2E-18 7E-17 L.L.D.+ Effluent Cone.* %Effluent ,..ci/mL ,..ci/mL Concentration IE-16 9E-14 5.21E+00 IE-16 3E-14 4.58E-Ol IE-16 9E-13 3.93E-02 2E-15 6E-13 1.81E+00 L.L.D.+ Effluent Cone.* %Effluent ,..cilmL flCi/mL Concentration IE-16 9E-14 4.63E+00 IE-16 3E-14 2.32E+00 IE-16 9E-13 1.97E-Ol 2E-15 6E-13 1.77E+00 Page 7 of 22 EN:RGY I .~ t._ , , 1• \ {_.1~ I ; www.energytab.com ~Em/i~Mt Sllre.IJ!I Helena, MT 877-472-0711 • Billings, MT 800·735-4489 • Casper, WY 888-235-0515 Gillette, WY 816-886·7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Air 2014 LabiD: c 14070123-003 Client Sample ID: BHV-4 Analyses Result Units TRACE METALS · IN AIR Uranium 6.2E-09 mgiL RADIONUCLIDES · IN AIR Lead 210 1.1 E-14 uCilmL Lead 210 precision (±) 1.9E-16 uCi/mL Lead 210 MDC 6.9E-17 uCilmL Radium 226 1.8E-15 uCilmL Radium 226 precision (±) 1.6E-17 uCilmL Radium 226 MDC 1.8E-18 uCilmL Thorium 230 7.0E-16 uCilmL Thorium 230 precision (±) 7.5E-17 uCil mL Thorium 230 MDC 8.5E-18 uCilml Uranium, Activity 4.2E-15 uCil mL RADIONUCLIDES · IN AIR-PER FILTER Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Uranium, Activity FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. 1460 pCiiFilter 25.5 pCiiFilter 9.5 pCiiFilter 244 pCiiFilter 2.1 pCiiFilter 0.25 pCiiFilter 95.7 pCi!Filter 10.3 pCiiFilter 1.2 pCiiFilter 572 pCiiFilter 137449163 L MDC -Minimum detectable concentration Qualifiers MCL/ RL QCL 1.5E-10 1.0E-16 0.20 Report Date: 07/29/14 Collection Date: 06/30/14 DateReceived: 07/02/14 Matrix: Filter Method Analysis Date I By SW6020 0711 0114 23:50 I elm E909.0 07127114 09:451 eli-cs E909.0 07127114 09:451 eli-cs E909.0 07127114 09:451 eli-cs E903.0 0711511419:131 dmf E903.0 07115114 19:13 1 dmf E903.0 07115114 19:13 1 dmf E908.0 07115114 09:06 I dmf E908.0 07115114 09:06 I dmf E908.0 07115114 09:061 dmf SW6020 07110114 23:50 I elm RADCALC 0712911414:261 smm RADCALC 0712911414:261 smm RADCALC 07129114 14:261 smm RADCALC 07129114 14:261 smm RADCALC 07129114 14:26 1 smm RADCALC 07129114 14:261 smm RADCALC 07129114 14:261 smm RADCALC 0712911414:261 smm RADCALC 0712911414:261 smm RADCALC 07129114 14:26 1 smm FIELD 06130114 00:00 I *** MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 8 of22 www.eneJiYiab.com Allll1b/ ~ Sillt:t I liZ Helena, r.rr 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 868-686-7115 • Rapid City, SD 888-872-1225 • College Station, TX 888-&90-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: July 29,2014 PROJECT: 2nd Quarter Air 2014 SAMPLE ID: BHV-5 Quarter/Date Sampled Concentration Radionuclide Air Volume J1Ci/mL C14040336-004 ""'U 4.74E-15 First Quarter 2014 23oTh 1.42E-15 Air Volume in mLs 226Ra 3.48E-15 1.35E+11 210Pb l.SOE-14 Quarter/Date Sampled Concentration Radionuclide Air Volume J1CilmL C14070123-004 nalu 8.18E-15 Second Quarter 2014 23oTh 1.34E-15 Air Volume in mLs 226Ra 1.76E-15 1.30E+ll 210Pb 1.42E-14 +LLD's are from NRC Reg. Guide 4.14 Counting Precision J1CilmL N/A 1E-16 8E-17 2E-16 Counting Precision J1CilmL N/A 2E-16 2E-17 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDC J1CilmL N/A 2E-17 IE-17 9E-17 MDC J1CilmL N/A 2E-17 2E-18 7E-17 L.L.D.+ Effluent Cone.* %Effluent J1CilmL J1CilmL Concentration 1E-16 9E-14 5.27E+00 1E-16 3E-14 4.73E+00 1E-16 9E-13 3.86E-01 2E-15 6E-13 2.51E+00 L.L.D.+ Effluent Cone.* %Effluent J1CilmL J1CilmL Concentration IE-16 9E-14 9.09E+00 1E-16 3E-14 4.47E+00 1E-16 9E-13 1.96E-Ol 2E-15 6E-13 2.37E+OO Page 9 of22 www.en&fRYiab.com EI\ERGY L J\ • ~ .._ 1-1 •• I ~I ~It ...... AMI/bl Elr»>iila SJnc. IIU Helena, MT 877-472-0711 • Billings, MT 800·735·4489 • Casper, WY 888-235-0515 Glllatta, WY 88&-688-7175 • Rapid C~, SD 888-672-1225 • College Station, TX 888-680-2218 LABORATORY ANAL VTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Air 2014 Lab ID: C14070123-004 Client Sample ID: BHV-5 Analyses Result Units TRACE METALS-IN AIR Uranium 1.2E-08 mgll RADIONUCLIDES -IN AIR Lead 210 1.4E-14 uCilmL Lead 210 precision (±) 2.1E-16 uCilmL Lead 210 MDC 6.9E-17 uCilmL Radium 226 1.8E-15 uCilmL Radium 226 precision (±) 1.5E-17 uCilmL Radium 226 MDC 1.7E-18 uCi/mL Thorium 230 1.3E-15 uCilmL Thorium 230 precision (±) 1.5E-16 uCilmL Thorium 230 MDC 2.0E-17 uCilmL Uranium, Activity 8.2E-15 uCilmL RADIONUCLIDES-IN AIR -PER FILTER Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Uranium, Activity FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. 1840 pCiiFilter 27.8 pCiiFilter 9.0 pCiiFilter 229 pCiiFilter 2.0 pCiiFilter 0.23 pCiiFilter 174 pCiiFilter 19.6 pCiiFilter 2.7 pCi!Filter 1060 pCiiFilter 129804469 L MDC -Minimum detectable concentration Qualifiers MCL/ RL QCL 1.5E-10 1.0E-16 0.20 Report Date: 07/29/14 Collection Date: 06/30/14 Date Received: 07/02/14 Matrix: Filter Method Analysis Date I By SW6020 07110114 23:531 elm E909.0 07127114 11:061 eli-cs E909.0 07127114 11 :06 I eli-cs E909.0 07127114 11 :06 I eli-cs E903.0 07116114 07:191 dmf E903.0 07116114 07:191 dmf E903.0 07116114 07:19 I dmf E908.0 07115114 09:061 dmf E908.0 07115114 09:061 dmf E908.0 07115114 09:061 dmf SW6020 07110114 23:531 elm RADCALC 0712911414:261 smm RADCALC 0712911414:261 smm RADCALC 0712911414:261 smm RADCALC 07129114 14:261 smm RADCALC 0712911414:261 smm RADCALC 0712911414:261 smm RADCALC 0712911414:261 smm RADCALC 0712911414:261 smm RADCALC 07129114 14:261 smm RADCALC 07129114 14:26 I smm FIELD 06130114 00:00 I *** MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 10 of 22 EI\ERGY ..... j ,,,•,'t••·l' www.energylab.com Allll1flal ~Sinn lim Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-&90-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: July 29, 2014 PROJECT: 2nd Quarter Air 2014 SAMPLE ID: BHV-6 Quarter/Date Sampled Concentration Radionuclide Air Volume ,..cilmL C14040336-005 ""u 8.92E-15 First Quarter 2014 z3oTh 7.68E-16 Air Volume in mLs 226Ra l.SOE-15 1.35E+ll 210Pb 1.61E-14 Quarter/Date Sampled Concentration Radionuclide Air Volume ,..cilmL C14070123-005 "''U 8.29E-15 Second Quarter 2014 230Th 5.35E-16 Air Volume in mLs 226Ra 6.72E-16 1.37E+11 zwPb 1.20E-14 +LLD's are from NRC Reg. Guide 4.14 Counting Precision 11ci!mL N/A 1E-16 4E-17 3E-16 Counting Precision ,..cilmL N/A SE-17 1E-17 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDC 11CilmL N/A 2E-17 6E-18 9E-17 MDC 11CilmL N/A 2E-17 2E-18 7E-17 L.L.D.+ Effluent Cone.* %Effluent ,..cilmL ,..cilmL Concentration 1E-16 9E-14 9.91E+00 1E-16 3E-14 2.56E+00 1E-16 9E-13 1.67E-01 2E-15 6E-13 2.69E+00 L.L.D.+ Effluent Cone.* %Effluent ,..cilmL ,..cilmL Concentration 1E-16 9E-14 9.21E+00 1E-16 3E-14 1.78E+00 1E-16 9E-13 7.47E-02 2E-15 6E-13 2.01E+00 Page 11 of 22 www.energylab.com EI\ERGY '\ I• j ... )( :n ANJytJrM ElwiiHct Sllcl II!Z Helena, MT 817·472-0111 • Billings, MT 800·735-4489 • Casper, WY 888-235·0515 Glllatta, WY 88&-686·7115 • Rapid City, SD 888-672·1225 • College Station, TX 888·690·2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Air 2014 LabiD: c 14070123-005 Client Sample ID: BHV-6 Analyses Result Units TRACE METALS ·IN AIR Uranium 1.2E-08 mg/L RADIONUCLIDES ·IN AIR Lead 210 1.2E-14 uCilmL Lead 210 precision (±) 2.0E-16 uCilmL Lead 210 MDC 6.9E-17 uCilmL Radium 226 6.7E-16 uCilmL Radium 226 precision (±) 9.5E-18 uCilmL Radium 226 MDC 1.8E-18 uCilmL Thorium 230 5.3E-16 uCilmL Thorium 230 precision (±) 7.6E-17 uCilmL Thorium 230 MDC 1.7E-17 uCilmL Uranium, Activity 8.3E-15 uCilmL RADIONUCLIDES-IN AIR -PER FIL TEA Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Uranium, Activity FIELD PARAMETERS Air Filtering Volume *** Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. 1650 pCiiFilter 27.1 pCi/Filter 9.5 pCiiFilter 92.4 pCiiFilter 1.3 pCiiFilter 0.25 pCiiFilter 73.5 pCiiFilter 10.4 pCiiFilter 2.4 pCiiFilter 1140 pCiiFilter 137419844 L MDC -Minimum detectable concentration Qualifiers MCL/ RL QCL 1.5E-10 1.0E-16 0.20 Report Date: 07/29/14 Collection Date: 06/30/14 DateReceived: 07/02/14 Matrix: Filter Method Analysis Date I By SW6020 07/1 0114 23:56 I elm E909.0 07127114 12:261 eli-cs E909.0 07127114 12:261 eli-cs E909.0 0712711412:261 eli-cs E903.0 07116114 07:191 dmf E903.0 07116114 07:191 dmf E903.0 07116114 07:191 dmf E908.0 07115114 09:061 dmf E908.0 07115114 09:061 dmf E908.0 07115114 09:061 dmf SW6020 07110114 23:561 elm RADCALC 07129114 14:261 smm RADCALC 07129114 14:261 smm RADCALC 0712911414:261 smm RADCALC 0712911414:261 smm RADCALC 07129114 14:261 smm RADCALC 07129114 14:261 smm RADCALC 0712911414:261 smm RADCALC 0712911414:261 smm RADCALC 0712911414:261 smm RADCALC 0712911414:261 smm FIELD 06130114 00:00 I *** MCL -Maximum contaminant level. ND -Not detected at the reporting limit. Page 12 of 22 EI\ERGY •• " ,-(,.' >~ H - www.energylab.com AHI1flal Elallllla Slm:t 1/ISZ Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 8&6-&8&· 7175 • Rapid City, SD 888-612-1225 • Collage Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: July 29,2014 PROJECT: 2nd Quarter Air 2014 SAMPLE ID: Blank Quarterffiate Sampled Concentration I Radionuclide Air Volume J.lCilmL C14040336-006 ""u 1.46E-17 First Quarter 2014 230Th 1.98E-18 Air Volume in mLs 226Ra 2.79E-18 1.36E+ll 2lDPb -1.20E-17 Counting Precision J.lCi/mL N/A IE-18 2E-18 4E-17 Note: This ~'1lmplc uses 136,000,000 L of air volume for comparison purpo~Cis. Quarterffiate Sampled Concentration Counting Radionuclide Precision Air Volume 11CilmL J.lCilmL C14070123-006 natu 1.90E-17 N/A Second Quarter 2014 23oTh 6.03E-18 2E-18 Air Volume in mLs 226Ra 5.02E-18 IE-18 1.36E+ll zwPb 6.18E-18 3E-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. +LLD's are from NRC Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCJ.1CilmL N/A 2E-18 2E-18 7E-17 MDCfJCilmL N/A 2E-18 IE-18 SE-17 L.L.D.+ Effluent Cone.* %Effluent J.1CilmL J.lCi/mL Concentration IE-16 9E-14 1.62E-02 IE-16 3E-14 6.60E-03 IE-16 9E-13 3.10E-04 2E-15 6E-13 -2.01E-03 L.L.D.+ Effluent Cone.* %Effluent J.lCi/mL J.1CilmL Concentration IE-16 9E-14 2.11E-02 IE-16 3E-14 2.01E-02 IE-16 9E-13 5.58E-04 2E-15 6E-13 1.03E-03 Page 13 of22 EI\ERGY I '\.LH •i .. l•i( I"IL www.energylab.com .,_,~sac. 1151 Helena, MT 877-472-0711 • Billings, MT 800-735·4488 • Caspar, WY 888-235·0515 Gillette, WY Bl&-&86-7175 • Rapid City, SD 888·872-1225 • College Station, 1X 888-690·2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Air 2014 Lab ID: C14070123-006 Client Sample ID: Blank Analyses TRACE METALS -IN AIR Uranium RADIONUCLIDES · IN AIR Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Uranium, Activity RADIONUCLIDES · IN AIR -PER FILTER Lead 210 Lead 210 precision (±) Lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Uranium, Activity FIELD PARAMETERS Air Filtering Volume ••• Field data provided by client Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result Units 0.0038 mgiL 8.4E-10 uCilmL 4.0E-09 uCilmL 6.6E-09 uCilmL 6.8E-1 0 uCilmL 1.4E-10 uCilmL 1.7E-1 0 uCilmL 8.2E-10 uCilmL 2.9E-10 uCilmL 2.4E-10 uCilmL 2.6E-09 uCilmL 0.84 pCiiFilter 4.0 pCi/Filter 6.6 pCi/Filter 0.68 pCii Filter 0.14 pCii Filter 0.17 pCiiFilter 0.82 pCiiFilter 0.29 pCiiFilter 0.24 pCiiFilter 2.6 pCiiFilter 1.0 L MDC -Minimum detectable concentration Qualifiers D u D u U -Not detected at minimum detectable concentration MCL/ RL CCL 0.000043 2.9E-11 0.20 Report Date: 07/29/14 Collection Date: 06/30/14 Date Received: 07/02/14 Matrix: Filter Method Analysis Date I By SW6020 07111114 00:17 I elm E909.0 07127114 13:46 I eli-cs E909.0 07127114 13:46 I eli-cs E909.0 07127114 13:46 I eli-cs E903.0 07116114 07:19 I dmf E903.0 07116114 07:19 I dmf E903.0 07116114 07:19 I dmf E908.0 07115114 09:06 I dmf E908.0 07115114 09:06 I dmf E908.0 07115114 09:06 I dmf SW6020 07111114 00:17 I elm RADCALC 07129114 14:26 I smm RADCALC 07129114 14:26 I smm RADCALC 07129114 14:261 smm RADCALC 07129114 14:26 I smm RADCALC 07129114 14:261 smm RADCALC 07129114 14:26 I smm RADCALC 07129114 14:26 I smm RADCALC 07129114 14:26 I smm RADCALC 07129114 14:26 I smm RADCALC 0712911414:26 I smm FIELD 06130114 00:00 I*** MCL -Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 14 of22 EN:RGY t ·, lt.•t··"•l •'i"l' • www.energylab.com AM/yfJrll Elf:INIIIct Slllu 11!1 Helena, MT 871·412·0711 • Billings, MT 800·735·4489 • Casper, WY 888·235·0515 Gillette, WY 861·688-71711 • Rapid City, SD 818-672-12211 • College Station,TX 881-690-2218 QAIQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Air 2014 Analyte Count Result Units Method: E903.0 Lab ID: C14070120-001AMS Radium 226 LabiD: C14070120·001AMSD Radium 226 Lab ID: LCS-41872 Radium 226 Lab ID: MB-41872 Radium 226 Radium 226 precision (±) Radium 226 MDC Lab 10: MB-41884 Radium 226 Radium 226 precision (±) Radium 226 MDC Qualifiers: RL -Analyte reporting limit. 3 3 MDC -Minimum detectable concentration Sample Matrix Spike 8.33E-07 pCi/L Sample Matrix Spike Duplicate 9.18E-07 pCi/L Laboratory Control Sample 21.2 pCi/L Method Blank 0.2 pCi!L 0.08 pCi!L 0.1 pCi/L Method Blank 0.05 pCi!L 0.07 pCi/L 0.1 pCi/L Report Date: 07/29/14 Work Order: C14070123 RL %REC Low Limit High Limit Run:G5000VV_140709B 90 70 130 Run:G5000VV_140709B 101 70 130 Run:G5000VV_140709B 97 80 120 Run: G5000VV_140709B Run:G5000VV_140709B NO -Not detected at the reporting limit. RPD RPDLimit Qual 9.6 Batch: R188757 07/15/1419:13 07/15/1419:13 13.7 07/15/1419:13 07/15/1419:13 07/16/14 07:19 u U -Not detected at minimum detectable concentration Page 15 of 22 EN:RGY 1 lt,,_,j ,•I :_::•IL'• www.energylab.com AllllyiJr:M Elwllrlla Slllc. IBU Helena, MT 877·472·0711 • Billings, MT 800-735-4489 • Casper, WV 888·235-0515 Gillette, WV 866-686-7175 • Rapid City, SO 888-672-1225 • Collage Station, TX 888-690-2218 QAJQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Air 2014 Analyte Count Result Units Method: E908.0 LabiD: C14070191-003AMS Thorium 230 Lab ID: C14070191-003AMSD Thorium 230 Lab ID: LCS-41884 Thorium 230 Lab ID: MB-41884 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Qualifiers: RL -Analyte reporting limit. 3 MDC - Minimum detectable concentration Sample Matrix Spike 1 .22E-05 pCi/L Sample Matrix Spike Duplicate 1.20E-05 pCi/L Laboratory Control Sample 16.4 pCi/L Method Blank 0.2 pCi/L 0.1 pCi/L 0.2 pCi!L Report Date: 07/29/14 Work Order: C14070123 RL %REC Low Limit High Limit RPD RPDLimit Qual Run: ALPHANAL YST_140709B 100 70 130 Run: ALPHANAL YST_140709B 98 70 130 1.7 Run: ALPHANAL YST_140709B 97 80 120 Run: ALPHANAL YST_140709B ND -Not detected at the reporting limit. Batch: 41884 07/15/14 09:06 07/15/14 09:06 30.8 07/15/14 09:06 07/15/14 09:06 Page 16 of22 EI\ERGY I ·,. l 1 •~,. I , )ill l ~- www.energylab.com AMiyflal~ .. 11111 Helena, MT 877·472·0711 • Billings, MT 800-735·4489 • Caspar, WY 888·235·0515 Gillette, WY 8&&-68&-7175 • Rapid City, SD 888-672-1225 • College Station, 1X 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Air 2014 Analyte Count Result Units Method: E909.0 Lab ID: MB-21598 Lead 210 Lead 21 0 precision (±) Lead 210 MDC Lab ID: LCS-21598 Lead 210 Lab ID: C14070123-001AMS Lead 210 Lab ID: C14070123-001AMSD Lead 210 Qualifiers: RL-Analyte reporting limit. 3 MDC -Minimum detectable concentration Method Blank -1 pCi/L 4 pCi/L 7 pCi/L Laboratory Control Sample 138 pCi/L Sample Matrix Spike 1.78E-05 pCi/L Sample Matrix Spike Duplicate 1.78E-05 pCi/L Report Date: 07/29/14 Work Order: C14070123 RL %REC Low Limit High Limit Run: SUB-T58010 Run: SUB-T58010 108 80 120 Run: SUB-T58010 121 70 130 Run: SUB-T5801 0 119 70 130 NO -Not detected at the reporting limit. RPD RPDLimit Qual 0.0 Batch: T_21598 07/27/14 01 :44 u 07/27/14 03:04 07/27/14 05:45 07/27/14 07:05 15.2 U -Not detected at minimum detectable concentration Page 17 of22 www.energylab.com ..,.,_,~Sin. IIU Helena, MT 877-472-0711 • Billings, MT 800-735·4489 • Casper, WV 888-235-0515 Gillette, WV 8&&-&8&-7175 • Rapid City, SD 818-&72-1225 • College Station, TX 888-680-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Air 2014 Report Date: 07/29/14 Work Order: C14070123 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: SW6020 Analytical Run: ICPMS2-C_14071 OA Lab ID: ICV Initial Calibration Verification Standard 07/10/14 13:24 Uranium 0.0505 mg/L LabiD: ICSA Interference Check Sample A Uranium 2.79E-05 mg/L Lab ID: ICSAB Interference Check Sample AB Uranium 7.10E-06 mg/L Method: SW6020 Lab ID: MB-41884 Method Blank Uranium 6E-05 mg/L Lab ID: LCS2-41884 Laboratory Control Sample Uranium 0.105 mg/L Lab ID: C14070123-005AMS Sample Matrix Spike Uranium 1.51 E-08 mg/L Lab ID: C14070123-005AMSD Sample Matrix Spike Duplicate Uranium 1.55E-08 mg/L Lab ID: C14070171-001 ADI L Serial Dilution Uranium 1.06E-10 mg/L Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. 0.00030 101 90 110 07/10/14 13:27 0.00030 07/10/14 13:30 0.00030 Batch: 41884 Run: ICPMS2-C_14071 OA 07/10/14 23:34 4E-05 Run: ICPMS2-C_14071 OA 07/10/14 23:38 4.3E-05 105 85 115 Run: ICPMS2-C_140710A 07/10/14 23:59 1.5E-10 75 125 A Run: ICPMS2-C_14071 OA 07/11/14 00:11 1.5E-10 75 125 2.1 20 A Run: ICPMS2-C_140710A 07/11/14 00:23 1.5E-10 20 A -The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. MDC -Minimum detectable concentration Page 18 of 22 EN:RGY • '{I • C1.oo'l ' www.energylab.com AII/Jfkl/~._,,!1 Helena, MT 877-472-0711 • Billings, MT 808·735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • Collage Station, TX 888-&90-2218 Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Corinne Wagner Reviewed by: Bl2000\swaldrop Reviewed Date: 7/3/2014 Shipping container/cooler in good condition? Custody seals intact on all shipping container(s)/cooler(s)? Custody seals intact on all sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.) Temp Blank received in all shipping container(s)/cooler(s)? Container/Temp Blank temperature: Water-VOA vials have zero headspace? Water-pH acceptable upon receipt? Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes D N/A'C Yes D Yes D C14070123 Date Received: 7/2/2014 Received by: dw NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD Carrier Next Day Air name: Not Present D Not Present D Not Present 0 Not Applicable 0 NoVOA vials submitted 0 Not Applicable 0 :::::::=====-----·---=======---==--==..-_-·:::::::==--==----_ --======---------==========-=--::.-=--========----------. Standard Reporting Procedures: Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Contact and Corrective Action Comments: None Page 19 of 22 . " Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: Energy Laboratories Contact: Garrin Palmer -=2::::39~3=-s~a..:::;lt:::;C::;r;.;.e;;.;ek~H:..::wy~------Ph: 435 678 4115 Casper, WY 82601 gpalmer@energy(uels.com Chain of Custody/Sampling Analysis Request Project Samplers Name Samplers S~nature 2nd Quarter Air 2014 Garrin Palmer I Time Sample ID Date Collected Collected Laboratory Analysis Requested BHV-1 3/31/14-6/30/14 NA U-NAT, TH-230. Ra-226, Pb-210 BHV-2 3/31/14-6/30/14 NA U-NAT, TH-230, Ra-226, Pb-210 BHV-4 3/31/14-6/30/14 NA U-NAT, TH-230, Ra-226. Pb-210 BHV-5 3/31/14-6/30/14 NA U-NAT, TH-230, Ra-226, Pb-210 BHV-6 3/31/14-6/30/14 NA U-NAT, TH-230, Ra-226, Pb-210 Blank 3/31/14-6730/14 NA U-NAT, TH-230, Ra-226, Pb-210 Comments: Send report to David Turk at PO Box 809 Blanding, UT 84511 Relinquished By:(Signature) Garrin Pal ~ Datemme Received By:(Signature) Date/Time 7/1/2014 1000 Date/Time Received By:(Signature) DeJ~e 4 - ATTACHMENTD AIR PARTICULATE LOADING GRAPHS AND SUPPORTING DATA 0 0 0 !=> ..... 0 0 0 ..... 0 0 0 ...... 0 0 0 ..... 0 0 0 ..... 0 0 0 0 1/5/2009 3/5/2009 5/5/2009 7/5/2009 9/5/2009 11/5/2009 1/5/2010 3/5/2010 5/5/2010 . l> + -· ., 7/5/2010 . "' !P r+ I 9/5/2010 DJ < I r+ ..... -· 11/5/2010 0 + ::::s 1/5/2011 "'0 !P DJ I 3/5/2011 < ., I r+ N -· 5/5/2011 n + c 7/5/2011 --DJ !P r+ I 9/5/2011 tD < I ""' r-11/5/2011 0 + DJ 1/5/2012 a. !P -· I 3/5/2012 ::::s < OQ I V'l 5/5/2012 - + 3 7/5/2012 OQ !P ......... I 9/5/2012 3 < I IN CTI 11/5/2012 - 1/5/2013 3/5/2013 5/5/2013 7/5/2013 9/5/2013 11/5/2013 1/5/2014 3/5/2014 5/5/2014 0 0 ~ 0 0 ..... ..... 0 0 ..... 0 0 ..... 0 0 0 0 0 0 0 1/5/2009 3/5/2009 5/5/2009 . 7/5/2009 . 9/5/2009 11/5/2009 1/5/2010 3/5/2010 5/5/2010 7/5/2010 . c:J :I: 9/5/2010 < I 11/5/2010 ..... -g 1/5/2011 QJ .., 3/5/2011 ~ -· n 5/5/2011 c t -QJ 7/5/2011 ~ tD OJ I 9/5/2011 < r- ~ 0 11/5/2011 QJ a.. -· 1/5/2012 j OQ 3/5/2012 - 5/5/2012 3 OQ 7/5/2012 ....... 3 9/5/2012 . w - 11/5/2012 1/5/2013 3/5/2013 5/5/2013 7/5/2013 . 9/5/2013 . 11/5/2013 1/5/2014 3/5/2014 . 5/5/2014 !=' !=' !=' ...... 0 0 ...... 0 0 ...... 0 0 ...... 0 0 0 0 0 0 0 1/5/2009 3/5/2009 5/5/2009 7/5/2009 9/5/2009 11/5/2009 1/5/2010 3/5/2010 5/5/2010 - 7/5/2010 c:J ::I: 9/5/2010 -< I 11/5/2010 -N ""C 1/5/2011 · OJ 3/5/2011 ~ -· n 5/5/2011 · c: + -OJ 7/5/2011 ~ It) OJ I 9/5/2011 < r- I 0 N 11/5/2011 · OJ c. -· 1/5/2012 ::::J OQ 3/5/2012 - 5/5/2012 3 OQ 7/5/2012 -....... 3 9/5/2012 -w -11/5/2012 1/5/2013 3/5/2013 5/5/2013 - 7/5/2013 - 9/5/2013 11/5/2013 - 1/5/2014 3/5/2014 5/5/2014 0 0 0 !=> 0 0 0 ..... ..... 0 0 0 ..... 0 0 0 ..... 0 0 0 ..... 0 0 0 0 1/5/2009 3/5/2009 5/5/2009 7/5/2009 9/5/2009 11/5/2009 1/5/2010 3/5/2010 5/5/2010 ... 7/5/2010 g:, :I: 9/5/2010 < I 11/5/2010 -~ "'C 1/5/2011 OJ .., 3/5/2011 ,.... -· n 5/5/2011 c + ~ -OJ 7/5/2011 ~ ,.... t1) OJ :I: 9/5/2011 < r- .J:,. 0 11/5/2011 OJ c. -· 1/5/2012 ::::s OQ 3/5/2012 - 5/5/2012 3 OQ 7/5/2012 ......... 3 9/5/2012 -w ~ - 11/5/2012 1/5/2013 3/5/2013 5/5/2013 7/5/2013 9/5/2013 ' 11/5/2013 1/5/2014 3/5/2014 5/5/2014 0 0 !=> 0 0 .... .... 0 0 .... 0 0 .... 0 0 0 0 0 0 0 1/5/2009 3/5/2009 5/5/2009 7/5/2009 9/5/2009 11/5/2009 1/5/2010 3/5/2010 5/5/2010 7/5/2010 O:J ::I: 9/5/2010 < I 11/5/2010 . U1 "'C 1/5/2011 Q) .., 3/5/2011 r1' -· n 5/5/2011 r:::: + - 7/5/2011 . Q) r1' tD OJ I 9/5/2011 < r- I 0 ln 11/5/2011 · Q) a. -· 1/5/2012 -::::J CJQ 3/5/2012 - 5/5/2012 3 CJQ 7/5/2012 ......... 3 9/5/2012 w - 11/5/2012 1/5/2013 3/5/2013 5/5/2013 7/5/2013 ~ 9/5/2013 11/5/2013 1/5/2014 3/5/2014 5/5/2014 . 0 0 9 1-' 0 0 1-' 0 0 1-' 0 0 1-' 0 0 0 0 0 0 0 1/5/2009 3/5/2009 5/5/2009 7/5/2009 9/5/2009 11/5/2009 1/5/2010 3/5/2010 .. 5/5/2010 7/5/2010 aJ :I: 9/5/2010 . < I 11/5/2010 . en ""0 1/5/2011 DJ ""'' 3/5/2011 r't' -· n 5/5/2011 s:::: + - 7/5/2011 DJ r't' t1) co :::c 9/5/2011 . < ~ &. 0 11/5/2011 DJ a. -· 1/5/2012 :::l C1Q 3/5/2012 - 5/5/2012 3 C1Q 7/5/2012 ........ 3 9/5/2012 w - 11/5/2012 1/5/2013 3/5/2013 5/5/2013 7/5/2013 9/5/2013 - 11/5/2013 1/5/2014 •. 3/5/2014 5/5/2014 Period: December 30, 2014 through March 31, 2014 (1st Quarter 2014) BHV-1 on stream o/o Week Filter Start tl Number Pate l 8398934 30-Dec-t3 2 8398931 06-Jan-14 3 8398926 13-Jan-14 4 8398915 20-Jan-14 5 8398913 27-Jan-14 6 8398908 03-Feb-14 7 8400197 10-Feb-14 8 8400195 17-Feb-14 9 8400185 24-Feb-14 10 8400183 03-Mar-14 II 8400174 10-Mar-14 12 8400171 17-Mar-14 13 8400162 24-Mar-14 Totals 91 BHV-2 on stream % Week Filter Start II Numbl!r Dale 1 8398935 30-Dec-13 2 8398930 06-Jan-14 3 8398925 13-Jan-14 4 8398916 20-Jan-14 5 8398912 27-Jan-14 6 8398907 03-Feb-14 7 8400198 10-Feb-14 8 8400194 17-Feb-14 9 8400186 24-Feb-14 10 8400182 03-Mar-14 11 8400175 10-Mar-14 12 8400170 17-Mar-14 13 8400163 24-Mar-14 Totals 91 BHV-4 on stream % Week Filter Start # Number Date 1 8398936 30-Dec-13 2 8398929 06-Jan-14 3 8398924 13-Jan-14 4 8398917 20-Jan-14 5 8398911 27-Jan-14 6 8398906 03-Feb-14 7 8400199 10-Feb-14 8 8400193 17-Feb-14 9 8400167 24-Feb-14 10 8400181 03-Mar-14 11 8400176 10-Mar-14 12 8400169 17-Mar-14 13 8400164 24-Mar-14 Totals 91 BHV-5 on stream % Week Filter Start 0 t # N b :urn er 11.8 1 8398937 30-0ec-13 2 8396926 06-Jan-14 3 8398923 13-Jan-14 4 8398918 20-Jan-14 5 8398910 27-Jan-14 6 8398905 03-Feb-14 7 8400200 10-Feb-14 a 8400192 17-Feb-14 9 8400188 24-Feb-14 10 8400180 03-Mar-14 11 8400177 10-Mar-14 12 8400168 17-Mar-14 13 8400165 24-Mar-14 Totals 91 100.0% Stop Date 6-Jan-14 13-Jan-14 20-Jan-14 27-Jan-14 3-Feb-14 10-Feb-14 17-Feb-t4 24-Feb-14 3-Mar-14 10-Mar-14 17-Mar-14 24-Mar-14 31-Mar-14 2184.0 100.0% Stop !:>ale 06-Jari-14 13-Jan-14 20-Jan-14 27-Jan-14 03-Feb-14 10-Feb-14 17-Feb-14 24-Feb-14 03-Mar-14 10-Mar-14 17-Mar-14 24-Mar-14 31-Mar-14 2184.0 99.2% Stop l:l_ate_ 06-Jan-14 13-Jan-14 20-Jan-14 27-Jan-14 03-Feb-14 10-Feb-14 17-Feb-14 24-Feb-14 03-Mar-14 10-Mar-14 17-Mar-14 24-Mar-14 31-Mar-14 2184.0 99.2% Stop D I a a 06-Jan-14 13-Jan-14 20-Jan-14 27-Jan-14 03-Feb-14 10-Feb-14 17-Feb-14 24-Feb-14 03-Mar-14 1D-Mar-14 17-Mar-14 24-Mar-14 31-Mar-14 2184.0 Gross Tare 4.3800 4.2984 4.4401 4.3256 4.4066 4.3245 4.4512 4.3263 4.4228 4.3208 4.3824 4.3206 4.4290 4.3376 4.4799 4.3329 4.4103 4.3091 4.4300 4.3473 4.5076 4.2810 4.5842 4.2655 5.7970 4.3069 4.547777 4.315115 Gross Tare 4.5'16'2 4.3505 4.5136 4.3039 4.5243 4.3209 4.6978 4.3268 4.5747 4.3372 4.3564 4.2699 4.4820 4.3175 4.5704 4.3233 4.4709 4.3266 4.4507 4.3294 4.5353 4.2767 4.6345 4.3048 5.0604 4.3138 4.568246 4.31548 Gress Tare 4.4091 4.3691 4.4670 4.3356 4.3786 4.3071 4.3474 4.2688 4.3973 4.2886 4.4070 4.3416 4.4187 4.3478 4.4759 4.3539 4.4052 4.3112 4.3661 4.2742 4.4616 4.3242 4.4627 4.3161 4.5536 4.2763 4.426938 4.3165 G rGSS T aro 4.3713 4.3000 4.4677 4.3326 4.4095 4.3131 4.4233 4.3122 4.4146 4.3053 4.4102 4.3462 4.4522 4.3381 4.4739 4.3328 4.4296 4.3329 4.4220 4.3368 4.5670 4.3213 4.5933 4.2636 4.8406 4.2750 4.482708 4.31615 Net 0.0816 0.1145 0.0821 0.1249 0.1020 0.0618 0.0914 0.1470 0.1012 0.0827 0.2266 0.3187 1.4901 0.2327 Net 0.1657 0.2097 0.2034 0.3710 0.2375 0.0865 0.1645 0.2471 0.1443 0.1213 0.2586 0.3297 0.7466 0.2528 Net 0.0400 0.1314 0,0715 0.0786 0.1087 0.0654 O.D709 0.1220 0.0940 0.0919 0.1374 0.1466 0.2773 0.1104 N t e 0.0713 0.1351 0.0964 0.1111 0.1093 0.0640 0.1141 0.1411 0.0967 0.0852 0.2457 0.3297 0.5656 0.1666 Stop Time 52612.7 52779.7 52946.3 53117.2 53286.2 53450.6 53619.3 53791.6 53953.8 54121.9 54293.4 54458.2 54627.9 Stop Time 62879:3 63046_0 63213.8 63382.9 63552.9 63717.2 63885.6 64057.6 64219.7 64388.2 64559.4 64727.5 64893.9 Stop Time 38114.1 38279.3 38445.8 36618.4 38784.1 38950.2 39118.8 39290.9 39453.8 39622.6 39792.8 39945.1 40116.1 Stop li InN! 61920.7 62085.9 62252.4 62425.0 62591.0 62756.7 62925.7 63097.9 63260.9 63429.2 63599.6 63752.0 63922.7 BHV-1 Start Time 52444.1 52612.7 52779.7 52946.3 53117.2 53286.2 53450.6 53619.3 53791.6 53953.8 54121.9 54293.4 54458.2 BHV-2 Start Time 62710.0 62879.3 63046.0 63213.8 63382.9 63552.9 63717.2 63885.6 64057.6 64219.7 64388.2 64559.4 64727.5 BHV-4 Start Ttme 37950.7 38114.1 38279.3 38445.6 36616.4 38784.1 38950.2 39118.8 39290.9 39453.8 39622.6 39792.8 39945.1 BHV-5 Start li 1me 61757.2 61920.7 62085.9 62252.4 62425.0 62591.0 62756.7 62925.7 63097.9 63260.9 63429.2 63599.6 63752.0 Total Time 10113.6 10023.0 9995.4 10255.2 10138.8 9862.2 10125.0 10336.8 9729.0 10089.6 10287.6 9886.8 10183.8 131026.8 Total Time 10154.4 10002.0 10073.4 10144.8 10196.4 9859.8 10104.0 10319.4 9729.6 10110.0 10269.6 10085.4 9987.0 131035.8 Total T IO'lB 9806.4 9911.4 9991.2 10355.4 9939.6 9968.4 10115.4 10329.0 9774.0 10126.2 10210.2 9140.4 10260.0 129927.6 Total n lffiB 9808.2 9912.0 9991.8 10354.2 9960.6 9946.2 10138.2 10329.0 9782.4 10096.8 10227.6 9144.0 10237.8 129928.8 Total Volume: 4.82E+06 Total Loading, Per Cent Liters mgfm3 0 n Slream 10,453,062 0.0078 100.3% 10,501,331 0.0109 99.4% 10,472,414 0.0078 99.2% 10,744,612 0.0116 101.7% 10,622,657 0.0096 100.6% 10,332,857 0.0060 97.8% 10,579,528 0.0086 100,4% 10,800,836 0.0136 102.5% 10,165,751 0.0100 96.5% 10,456,827 0.0079 100.1% 10,603,771 0.0214 102.1% 10,190,653 0.0313 98.1% 10.496,781 0.1420 101.0% 136,421,082 0.0222 100.0% Total Volume: 4.82E+06 Total Loading, Per Cent Liters I mglm3 On Stream 10,495,232 0.0158 100_7% 10,479,329 0.0200 99.2% 10,554.136 0.0193 99.9% 10,628,944 0.0349 100.6% 10,683,006 0.0222 101.2% 10,330,343 0.0084 97.8% 10,557,585 0.0156 100.2% 10,782,655 0.0229 102.4% 10,166,378 0.0142 96.5% 10,477,970 0.0116 100.3% 10,585,218 0.0244 101.9% 10,395,357 0.0317 100.1% 10,293,933 0.0725 99.1% 136.430 085 0.0241 100.0% Total Volume: 4.78E+06 Total Loading. Per Cent Uters roolm3 On Stream 10,135,551 0.0039 97.3% 10,384,405 0.0127 96.3% 10.468,013 0.0068 99.1% 10,849,594 0.0072 102.7% 10.413,951 0.0104 98.6% 10,444,125 0.0063 98.9% 10,569,497 0.0067 100.4% 10,792,686 0.0113 102.5% 10,212,771 0.0092 97.0% 10,494,759 0.0088 100.5% 10,523,992 0.0131 101.3% 9,421,314 0.0156 90.7% 10,575,323 0.0262 101.8% 135,285,-983 0.0106 99.2% Total Volume: 4.78E+06 Total L't 1 ets 10,137A11 10,385,034 10,468,642 10,848,337 10,435,953 10,420,866 10,593,321 10,792,686 10,221,548 10.464.289 10,541,927 9.425,025 10.552,441 135,287,479 Loading, Per Cent I 3 0 S!r mg,m n earn 0.0070 97.3% 0.0130 98.3% 0.0092 99.1% 0.0102 102.7% 0.0105 98.8% 0.0061 98.7% 0.0108 100.6% 0.0131 102.5% 0.0095 97.0% 0.0081 100.2% 0.0233 101.5% 0.0350 90.7% 0.0536 101.6% 0.0161 99.2% Page 1 SCF M 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 SO -M 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36,9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 Period: December 30, 2014 through March 31, 2014 (1st Quarter 2014) BHV-6 on stream % Week Filter Start IJ. Number Date 1 8398938 30-Dec-13 2 8398927 06-Jan-14 3 8398922 13-Jan-14 4 8398919 20-Jan-14 5 8398908 27-Jan-14 6 8398904 03-Feb-14 7 8398901 10-Feb-14 8 8400191 17-Feb-14 9 8400189 24-Feb-14 10 8400179 03-Mar-14 11 8400178 10-Mar-14 12 8400167 17-Mar-14 13 8400166 24-Mar-14 Totals 91 ALL BHV on stream o/o Week # BlBnkS Start Date 1 8398932 30-Dec-13 2 8398921 06-Jan-14 3 8398920 13-Jan-14 4 8398914 20-Jan-14 5 8398903 27-Jan-14 6 8398902 03-Feb-14 7 8400196 10-Feb-14 8 8400190 17-Feb-14 9 8400184 24-Feb-14 10 8400173 03-Mar-14 11 8400172 10-Mar-14 12 8400161 17-Mar-14 13 8400160 24-Mar-14 Totals 91 99.1% Stop Date 06-Jan-14 13-Jan-14 20-Jan-14 27-Jan-14 03-Feb-14 10-Feb-14 17-Feb-14 24-Feb-14 03-Mar-14 10-Mar-14 17-Mar-14 24-Mar-14 31-Mar-14 2f84.0' 99.5% Stop Dale 06-Jan-14 13-Jan-14 20-Jan-14 27-Jan-14 03-Feb-14 10-Feb-14 17-Feb-14 24-Feb-14 03-Mar-14 10-Mar-14 17-Mar-14 24-Mar-14 31-Mar-14 2184.0 Gross 4.43"94 4.4810 4.4235 4.4576 4.4825 4.3672 4.4581 4.4266 4.4495 4.4052 4.5073 4.5210 4.6986 4.470577 Net 4.3495 4.3245 4.2957 4.2864 4.3409 4.3619 4.3532 4.3618 4.3147 4.3199 4.3180 4.2386 4.3099 4.3212 BHV-6 Stop Start Tare Net 11me Thne 4.3331 0.1063 10316.0 10152.6 4.2748 0.2062 10481.2 10316.0 4.3271 0.0964 10647.7 10481.2 4.3269 0.1307 10820.3 10647.7 4.3352 0.1473 10986.0 10820.3 4.3198 0.0474 11151.7 10986.0 4.3317 0.1264 11320.7 11151.7 4.2843 0.1423 11492.9 11320.7 4.3580 0.0915 11655.8 11492.9 4.3430 0.0622 11824.5 11655.8 4.2933 0.2140 11994.4 11824.5 4.2938 0.2272 12147.1 11994.4 4.3105 0.3881 12318.1 12147.1 4.31781 0.1528 Page2 Total Volume: 4. 78E+06 Total Total Loading, Per Cent Time Uters ma/m3 On Stream SCFM 9802.8 10,131,830 0.0105 97.3% 36.5 9910.2 10,383,148 0.0199 98.3% 37.0 9991.2 10,468,013 0.0092 99.1% 37.0 10354.2 10,848,337 0.0120 102.7% 37.0 9941.4 10,415,837 0.0141 98.6% 37.0 9945.6 10,420,237 0.0045 98.7% 37.0 10138.8 10,593,948 0.0119 100.6% 36.9 10329.0 10,792,686 0.0132 102.5% 36.9 9778.2 10,217,160 0.0090 97.0% 36.9 10122.0 10,490,406 0.0059 100,4% 36.6 10194.0 10,507.295 0.0204 101.1% 36.4 9157.2 9,438,630 0.0241 90.8% 36.4 10260.6 10,575,941 0.0367 101.8% 36.4 129925.2 135.283.468 0.0147 99.1% 36.8 'Period: March 31, 2014 through, July 2, 2014 (2nd Quarter 2014) Page 1 # I 2 3 4 s 6 7 8 9 10 II 12 13 Week # 1 2 3 4 5 6 7 8 9 10 11 12 13 Week 11: 1 2 3 4 5 6 7 8 9 10 11 12 13 Week It 1 2 3 4 5 6 7 8 9 10 11 12 13 BHV-1 on stream% Number Date 8400159 31-Mar-14 8400150 07-Apr-14 8400147 14-Apr-14 8400141 21-Apr-14 8400132 28-Apr-14 8400128 05-May-14 8400120 12-May-14 8400117 19-May-14 8400111 26-May-14 8400102 02-Jun-14 8951299 09-Jun-14 8951290 16-Jun-14 8951286 23-Jun-14 Totals 91 BHV-2 on stream % Filter Start Number Date 8400158 31-Mar-1 4 8400151 07-Apr-14 8400146 14-Apr-14 8400140 21-Apr-14 8400133 28-Apr-14 8400129 05-May-14 8400121 12-May-14 8400116 19-May-14 8400110 26-May-14 8400103 02-Jun-14 8951298 09-Jun-14 8951291 16-Jun-14 8951285 23-Jun-14 Totals 91 BHV-4 on stream% Filter Start Numbcer Date 8400f57 31-Mar-14 8400152 07-Apr-14 8400145 14-Apr-14 8400139 21-Apr-14 8400134 28-Apr-14 8400127 05-May-14 8400122 12-May-14 8400115 19-May-14 8400109 26-May-14 8400104 02-Jun-14 8951297 09-Jun-14 8951292 16-Jun-14 8951284 23-Jun-14 T otals 91 BHV-5 on stream % Filter Start Numbor Date 8400156 31-Mar-14 8400153 07-Apr-14 8400144 14-Apr-14 8400138 21-Apr-14 8400135 28-Apr-14 8400126 05-May-14 8400123 12-May-14 8400114 19-May-14 8400108 26-May-14 8400105 02-Jun-14 8951296 09-Jun-14 8951293 16-Jun-14 8951283 23-Jun-14 Totals 91 98.8% Oate Gro'ss Tare Net 7-Apr-14 4.8063 4.2971 0.5092 14-Apr-14 4.6346 4.3412 0.2934 21-Apr-14 4.8566 4.3218 0.5348 28-Apr-14 4.7298 4.1975 0.5323 S-May-14 4.7308 4.2644 0.4664 12-May-14 4.5391 4.2729 0.2662 19-May-14 4.5319 4.2590 0.2729 26-May-14 4,6629 4,2162 0.4467 2-Jun-14 4.4344 4.1909 0.2435 9-Jun-14 4.4623 4.2810 0,1813 16-Jun-14 4.9799 4.5222 0.4577 23-Jun-14 5.1655 4.5152 0.6503 30-Jun-14 4.7708 4.5006 0.2702 2184.0 4.715762 4.321538 0.3942 99.9% Stop Date Gross Tare Net 07-Apr-14 4.5918 4.2783 0.3135 14-Apr-14 4.6736 4.2849 0.3887 21-Apr-14 4.7082 4.3398 0.3684 28-Apr-14 4.8015 4.3331 0.4684 05-May-14 4.5305 4.2645 0.2660 12-May-14 4.7203 4.2497 0.4706 19-May-14 4.4577 4.1937 0,2640 26-May-14 4.7318 4.2443 0.4875 02-Jun-14 4.5476 4.2523 0.2953 09-Jun-14 4.5685 4.2733 0.2952 16-Jun-14 4.9192 4.5293 0.3899 23-Jun-14 5.2519 4.5034 0.7485 30-Jun-14 4.7890 4.4948 0.2942 2184.0 4.71473'8 4.32626 0.3885 99.8% Stop Date Gross Tare Net 07-Apr-14 4.5233 4.3132 0.2101 14-Apr-14 4.4959 4.3393 0.1566 21-Apr-14 4.4564 4.3082 0.1482 28-Apr-14 4.6815 4.3499 0.3316 05-May-14 4.4871 4.2187 0.2684 12-May-14 4.4879 4.2615 0.2264 19-May-14 4.4076 4.2468 0.1608 26-May-14 4.4733 4.2211 0.2522 02-Jun-14 4.3529 4.2575 0.0954 09-Jun-14 4.2784 4.2379 0.0405 16-Jun-14 4.6324 4.5053 0.1271 23-Jun-14 4.9105 4.4993 0.4112 30-Jun-14 4.6131 4.4796 0.1335 2184.0 4.5231 4.32602 0.1971 94.3% Stop Date GraS$ Tare Nee 07-Apr-14 4.5511 4.3099 0.2412 14-Apr-14 4.5757 4.3419 0.2338 21-Apr-14 4.4912 4.3236 0.1676 28-Apr-14 4.7322 4.3297 0.4025 05-May-14 4.6506 4.2623 0.3883 12-May-14 4.7119 4.2860 0.4259 19-May-14 4.4569 4.2558 0.2011 26-May-14 4.5856 4.2085 0.3771 02-Jun-14 4.4269 4.2320 0.1969 09-Jun-14 4.5284 4.2599 0.2685 16-Jun-14 4.8025 4.5117 0.2908 23-Jun-14 5.0595 4.4744 0.5851 30-Jun-14 4.7259 4.5147 0.2112 2184.0 4.-6-38492 4.33157 0.3009 BHV-1 Total Volume: 4.80E+06 Loading Percent Stop Time Start Time Total Time Total Liters mg/m3 On Stream SCFM 54795.5 54961.7 55130,8 55297.0 55467.1 55609.4 55777.7 55969.6 56115.1 56280.9 56448.8 56641.4 56784.9 Stop Time 65061 .7 65228.1 65397.1 65564.4 65733.1 65899.6 66068.2 66260.2 66405.4 66571.4 66739.4 66932.0 67075.4 Stop Tlme 40283.2 40448.5 40616.8 40784.0 40952.7 41119.5 41287.9 41480.0 41623.7 41790.7 41958.5 42151.3 42296.3 Stop Time 64090.2 64255.4 64423.8 64591.0 64759.8 64926.4 65094.8 65286.5 65309.6 65476.5 65644.0 65836.8 65981.8 54627.9 54795.5 54961.7 55130.8 55297.0 55467.1 55609.4 55777.7 55969.6 56115.1 56280.9 56448.8 56641.4 BHV-2 Start ,., m& 64893.9 65061.7 65228.1 65397.1 65564.4 65733.1 65899.6 66068.2 66260.2 66405.4 66571.4 66739.4 66932.0 BHV-4 Start Tlrne 40116.1 40283.2 40448.5 40616.8 40784.0 40952.7 41119.5 41287.9 41480.0 41623.7 41790.7 41958.5 42151.3 BHV-5 Start Tlmll 63922.7 64090.2 64255.4 64423.8 64591.0 64759.8 64926.4 65094.8 65286.5 65309.6 65476.5 65644.0 65836.8 10054.8 9972.0 10144.8 9972.0 10206.0 8537.4 10096.2 11518.8 8727.6 9945.6 10076,4 11557.8 8607.0 129416.4 Total Time 10065.6 9981.0 10142.4 10036.2 10121.4 9995.4 10113.6 11519.4 8711.4 9961.2 10077.6 11556.6 8605.2 130887 Total Tlme 10025.4 9920.4 10097.4 10032.6 10121.4 10005.6 10103.4 11525.4 8622.6 10018.2 10072.2 11567.4 8698.2 130810.2 Total TlfTIB 10050.6 9912.0 10102.2 10033.8 10128.6 999'7.8 10105.2 11502.0 1386.0 10012.8 10050.0 11567.4 8697.6 123546 10,738,617 0.0474 99.8% 10,650,186 0.0275 98.9% 10,834,738 0.0494 100.6% 10,650,186 0.0500 98.9% 10,900,100 0.0428 101.2% 8,985,958 0.0296 84.7% 10,626,658 0.0257 100.2% 12,124,002 0.0368 114.3% 9,186,151 0.0265 86.6% 10,219,152 0.0177 98.7% 10,353,550 0.0442 100.0% 11,875,695 0.0548 114.7% 8,843.734 0.0306 85.4% 135,988,725 0.0372 98.8% Total Volume: 4.86E+06 Total Loading, Per Cent !-.item 1TIIl(m3 On Stream 10,750,151 0.0292 99.9% 10,659,798 0.0365 99.0% 10,832,174 0.0340 100.6% 10,718,752 0.0437 99.6% 10,809,746 0.0246 100.4% 10.520,562 0.0447 99.2% 10,644,972 0.0248 100.3% 12,124,633 0.0402 114.3% 9,169,100 0.0322 86.4% 10,235,181 0.0288 98.8% 10,354,783 0.0377 100.0% 11,874,462 0.0630 114.6% 8,841,885 0.0333 85.4% 137,536,199 0.0364 99.9% Total Volume: 4.85E+06 Total t Uens 10,707,217 10,595,076 10,784,114 10,714,907 10,809,746 10,531,298 10,634,236 12,130,949 9,075,634 10,293,749 10,349,234 loading, Per Cent mt~frn3 On Stream 0.0196 99.5% 0.0148 98.4% 0.0137 100.2% 0.0309 99.5% 0.0248 100.4% 0.0215 99.3% 0.0151 100.2% 0.0208 114.3% O.D105 85.5% 0.0039 99.4% 0.0123 99.9% 37.7 ill ---- . ____E;!__- 37.7 -37.7 ·- •• 37.2 -- 37.2 , ____ 37.2 37.2 36.3 36.3 36.3 36.3 37.1 SCFM r---m---37.7 ~-m- ~3'7:i'"" . 37:7-'37.2- • 37.2 - 37.2 -372 "36.3 36.3 -36.3 --= 36.3 37.1 SCFM 37.7 37.7 -- 37.7 ~~~ 37.7 ·-----37.2 ,_ 37.2 . -J 7.2 . .... B2o.. ... 36.3 ·---36.3 11,885,559 0.0346 114.8% I' 36.3 8,937,443 0.0149 86.3% 36.3 137,449,163 0.0183 99.8% I 37.1 Total Volume: 4.58E+06 Total loading, Per Cent Uters rna/m3 On Stream SCFM 10,734,131 0.0225 99.7% 1-..I!..:2._ -10,586,105 0.0221 98.3% 37.7 10,789,240 0.0155 100.2% 37.7 10,716,189 0.0376 99.5% "31:1- 10,817,436 0.0359 100.5% .. _"37J • .. 10,523.088 0.0405 99.2% 37.2 •• J 7.2 -10,636,131 0.0189 100.2% ·----12,106,319 0.0311 114.1% 37.2 1,458,821 0.1350 13.7% ---n2-- 10,288,200 0.0261 99.3% 363 10,326,424 0.0282 99.7% -36.3 -• 11,885,559 0.0492 114.8% ~. 36.~- 8'.93b,826 0.0236 86.3% 36.3 129,804,469 0.0374 94.3% 37.1 Period: March 31,2014 through, July 2, 2014 (2nd Quarter 2014) BHV-6 on stream% Week Filter Start # Number Dale 1 8400155 31-Mar-14 2 6400154 07-Apr-14 3 8400143 14-Apr-14 4 8400137 21 -Apr-14 5 8400136 28-Apr-14 6 6400125 05-May-14 7 6400124 12-May-14 8 8400113 19-May-14 9 6400107 26-May-14 10 8400106 02-Jun-14 11 8951295 09-Jun-14 12 8951288 16-Jun-14 13 8951282 23-Jun-14 Totals 91 ALL BHV on stream % Week # Blanks Start Date 1 8400149 31-Mar-14 2 8400148 07-Apr-14 3 8400142 14-Apr·14 4 8400131 21-Apr-14 5 8400130 28-Apr-14 6 8400119 05-May-14 7 8400118 12-May-14 8 8400112 19·May-14 9 8400101 26-May-14 10 8951300 02-Jun-14 11 8951289 09-Jun-14 12 8951287 16-Jun-14 13 8.951276 2.3-Jun-14 Totals 91 99.6% Stop Date 07-Apr-14 14-Apr-14 21-Apr-14 28-Apr-14 05-May-14 12-May-14 19-May-14 26-May-14 02-Jun-14 09-Jun-14 16-Jun-14 23-Jun-14 3Q-Jun-14 2184.0 98.5% Stop Date 07-Apr·14 14-Apr-14 21·Apr-14 28-Apr-14 05-May-14 12-May-14 19-May-14 26--May-14 02-Jun-14 09-Jun-14 16-Jun-14 23-Jun-14 ~O-Jun·14 2184.0 Gross 4.5391 4.4706 4.5014 4.5892 4.5218 4.5757 4.3876 4.5858 4.4341 4.4956 4.8099 4.9500 4.6910 4.580923 Net 4.3292 4.3029 4.3273 4.2278 4.2608 4.2455 4.1979 4.2549 4.2409 4.5127 4.5030 4.4919 4.5445 4.3415. Stop Tare Net Tlme 4.2920 0.2471 12485.2 4.2914 0.1792 12652.2 4.3430 0.1564 164.1 4.2897 0.2995 331 .3 4.2683 0.2535 500.0 4.2441 0.3316 666.7 4.2126 0.1752 835.2 4.2617 0.3241 1027.2 4.2544 0.1797 1171.1 4.2648 0.2308 1336.0 4.5055 0.3044 1505.8 4.5046 0.4454 1698.4 4.5023 0.1887 1845.7 4.32572 0.2552 Page2 BHV-6 Total Volume: 4.85E+06 Start Total Total Loading, Per Cent Tlma nme Liters mg/m3 On Stream SCFM 12318.1 10026.6 10,708.499 0.0231 99.5% ~-12465.2 10020.0 10,701,450 0.0167 99.4% 37.7 0.0 9844.8 10,514,335 0.0151 97.7% --3.,-:;----·-----164.1 10032.6 10,714,907 0.0280 99.5% 37.7 331.3 10124.4 10,812,950 0.0234 100.4% "'3-[i "'' 500.0 10002.0 10,527,509 0.0315 99.2% "37.2 " 666.7 10!05.8 10.636,762 0.0165 100.3% -37.2·- 835.2 11524.2 12,129,665 0.0267 114.3% 37.2 - 1027.2 8630.4 9,083,844 0.0196 65.6% 37.2 1171.1 10014.0 10,289,433 0.0224 99.3% 36.3 1338.0 10071.0 10,348.001 0.0294 99.9% ")"6.3 - 1505.8 11557.2 11,875,079 0.0375 114.7% 36.3 1698.4 8834.4 9,077.389 0.0208 87.6% 36.3 130787.4 137,419,844 0.0239 99.8% 37.1 ATTACHMENT E ENVIRONMENTAL GAMMA GRAPHS AND SUPPORTING DATA I White Mesa Mill Ambient Gamma Levels Over Time BHV-=11 50.00 --------------------------------------------------------------------------------------------------------------------~ 45.00 ~1--------------------------------------------------------------------------------------------------------------~ 40.00 ~----------------------------------------------------------------------------------------------------------l 35.00 I 30.00 ..... Q) t ca 25.00 :::::1 o-........ E Q) a: 20.00 E 15.00 10.00 II I 5.00 1 • I • II • ~ 0.00 ~~~ , .. ~ -I ' 9130it9st 91aol19sa 91aol19ss 9130it9B? 9130it9B9 9130it99t 91aolt993 91aolt99s 9130it99? 9130it999 913ol2oot 91aol2oo3 9130I2oos 91aol2oo? 913ol2oo9 9130I2ott 91aol2ot3 Background (BHV-3) Subtracted from BHV-1 I ......-.series1 I I White Mesa Mill Ambient Gamma Levels Over Time BHV-21 50.00~----------------------------------------------~-------------------------------------------------------, 45.00 +-------------------------------------------------------------------------------------------------------~ 40.00 +-------------------------------------------------------------------------------------------------------~ 35.00 +-------------------------------------------------------------------------------------------------------~ 30.00 ,_ CD t ctS ::::l 0" 25.00 -E CD 0: E 20.00 15.00 +--------------------------------------------------------------------------------------------------------1 10.00 +---------------~~----------------------------------------------------------------------------------------~ 5.00 i R H II W - o.oo i'At,¥~··~=-t •••··•·--~·~~VSbt-ti· --.. :rtar -....... ~.-~·V:JAIStllt ·~··*Wi .-.se .ww:.:,.-. 30-sep.81 30-sep.e9 30-sep.97 3o.seP-Os 3o.sep.13 Background (BHV-3) Subtracted from BHV-2 I --+--BHV-2 -1 ..... Q) t <U ::::J -!2"" E Q) a: E I White Mesa Mill Ambient Gamma Levels OverTime BHV-3] 50.00 ~------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------~ 45.00 +-------------------------------------------------------------------------------------------------~~----------------------------1 40.00 -ll------------tll---------------------------------1 ~ 35.00r-----------------------------------~--------------------------------------------1t--------------~~--~lrj~l-~~------------__j ~u.~ t-------------------~~-----~,_-----~~----- 4 ~ 25.00i~l~11~~;-~~-:t\~rt-1'~~~Jtj~~fJ~i:~~1\~~~--il~~--~--~~~~-~~~~~~~JJ ·rit-----~U I 2o.oo ~--------~r1~~~---Wf4~~~~--------------------~~---U-ll~~ ~~1-------------------~----~--------1 15.00 -j ~----IL_----1 4 10.00~!--------------------------------------------------------------------------------------------------------------------~ 5.00 i I o.ooL---------------r---------------------~----------------------------------------~--------------~------------------------------~ 3a..seP-Bt 3n ~ 3n ~ 3o.8 3o ... ~eP-83 ~eP-85 eP-87 vep.89 30-sep.g1 3o.sep.93 ao.8 3a..s 3o.s 3o.8 ep.gs ep.g7 ep.gg ep.ot 3o.sep.o3 3o-s 3o_.. 3o.8 3o-s ep.os vep.07 ep.og ep.11 30-sep.13 --BHV-3 I White Mesa Mill Ambient Gamma Levels Over Time BHV-4 1 50.00,-----------------------------------------------------------------------------------------------------------------------------, 45.00 1-----------------------------------------------------------------------------------------------------------------------------------, 40.00 +---------------------------------------------------------------------------------------------------------------------------~ 35~o 1 30.00 ..... Q) t: 25.00 ctl :::::l -!2"" E Q) 0: 20.00 E 15.00 10.00 5.oo -1--.-\-....a-\-l"f W _ H _ I o.oo ..,_ " -, M ~s ~s ~s ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ eP-87 ep.83 ep-as "SP-87 ep.ag ep.g1 ep.g3 ep.gs ep.g7 ep.gg eP·Ot ep.03 ep.os ep.07 ep.Og ep.11 ep.13 Background (BHV-3) Subtracted from BHV-4 --BHV-4 I White Mesa Mill Ambient Gamma Levels Over Time BHv:s] 50.00~--------------------------------------------------------------------------------------------------~ 45.00 +-----------------------------------------------------------------------------------------------------4 40.00 +-----------------------------------------------------------------------------------------------------~ 35.oo L ----------------------------------------l 30.00 ...... Q) t::: as :::J 0" 25.00 -E Q) a: E 20.00 15.00 +---------------------------------------------------------------------------------------------------------~ 10.00l_---------------------------------------------------------1t----.--~=---------------------~--------l 5.oo ~ I I 1e a. t•a n..-..,.. Ian. I I a -.a I I :l I I .L I I W I -lf-1-+\---------:e-J.d o.oo •• -, .._ 1 ~•• , e e ·• • e • · 1 •.., -1 30-Sep-81 30-seP-84 30-SeP-87 30-Sep.90 30-sep.g3 30-Sep.96 3o..sep.g9 3o..sep.o2 30-Sep-o5 3o..seP-oa 30-seP-1t Background (BHV-3) Subtracted from BHV-5 'I ~BHV-5 I I White Mesa Mill Ambient Gamma Levels Over Time BHv:s l 50.00 45.00 40.00 35.00 30.00 ..... Q) t ro 25.00 -:::s 0" --E Q) a: 20.00 E 15.00 -- 10.00 5.00 0.00 ... ~ _.r-.. .~ ~~ -----~-~ft ~ft -s ~ft -s -s ~ft -s ~ft -s -s -s -s -s ~ft -s ~eP-81 """'eP-83 """'eP-85 eP-8-, --..eP-89 ep_91 ep.93 """'ep.95 ep.97 """'ep_99 eP-01 ep-o3 eP-05 eP-0-, eP-og """'ep.11 ep.13 Background (BHV-3) Subtracted from BHV-6 I -~ I Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 51 52 53 64 White Mesa Mill First Quarter 2014 Environmental Spherical Gamma Monitor Results Location Administration Vault V205 Control Room BHV-6 Ore Star. -Barrel Area Vanadium Precip.Area Yellowcake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room Trammel Screen (ore pad) North East Corner Ore Pad Met. Lab Filter Press Room BHV-1 BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scale house Sample Plant (OBS) Front Gate AF -Barrel Dump Station AF Circuit -South AF Circuit-North North Control # 1 North Control # 2 CaF2 Barrel Dump Station - Operator Station KF Barrel Dump Station Date Issued 1/2/2014 1/2/2014 11212014 112/2014 112/2014 112/2014 1/2/2014 112/2014 11212014 1/2/2014 11212014 11212014 11212014 11212014 1/2/2014 11212014 112/2014 112/2014 11212014 112/2014 1/2/2014 112/2014 1/2/2014 112/2014 112/2014 1/2/2014 11212014 112/2014 112/2014 1/2/2014 11212014 112/2014 1/212014 112/2014 11212014 1/212014 1/2/2014 1/212014 112/2014 112/2014 1/2/2014 112/2014 Total Days Badge at Date Returned WMM 3/27/2014 84 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/2712014 3/27/2014 3/27/2014 3/2712014 3127/2014 3/27/2014 3/2712014 3/27/2014 3127/2014 3/27/2014 3/27/2014 312712014 3/2712014 3127/2014 3/2712014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3127/2014 312712014 3/27/2014 3127/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3127/2014 3/27/2014 3/2712014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 84 Mean Ambient Dose Equivalent 36.5 44.1 33.2 461.5 283.1 125.3 322.6 0 70.6 113 295.3 87.3 152.7 32 28.9 28.1 31.5 32.6 314.9 56.8 70.1 50.8 37.8 77.2 0 0 160.1 55.5 97.8 46.9 342.8 183.7 180.5 179 0 86.8 114.5 32.3 0 107.3 mRem/ mRem/ hour Day 0.02 0.435 0.02 0.02 0.23 0.00 0.14 0.06 0.16 0.00 0.04 0.06 0.15 0.04 0.08 0.02 0.01 0.01 0.02 0.02 0.16 0.03 0.03 0.03 0.02 0.04 0.00 0.00 0.08 0.03 0.05 0.02 0.17 0.09 0.09 0.09 0.00 0.04 0.06 0.00 0.02 0.00 0.05 0.525 0.395 5.494 0.000 3.370 1.492 3.840 0.000 0.840 1.345 3.515 1.039 1.818 0.381 0.344 0.335 0.375 0.388 3.749 0.676 0.835 0.605 0.450 0.919 0.000 0.000 1.906 0.661 1.164 0.558 4.081 2.187 2.149 2.131 0.000 1.033 1.363 0.000 0.385 0.000 1.277 mRem/ Week 3.04 3.68 2.77 38.46 0.00 23.59 10.44 26.88 0.00 5.88 9.42 24.61 7.28 12.73 2.67 2.41 2.34 2.63 2.72 26.24 4.73 5.84 4.23 3.15 6.43 0.00 0.00 13.34 4.63 8.15 3.91 28.57 15.31 15.04 14.92 0.00 7.23 9.54 0.00 2.69 0.00 8.94 Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 51 52 53 64 White Mesa Mill Second Quarter 2014 Environmental Spherical Gamma Monitor Results Location Administration Vault V205 Control Room BHV-6 Ore Stor.-Barrel Area Vanadium Precip.Area Yellowcake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room Ore pad -decontamination pad North East Corner Ore Pad Met. Lab Filter Press Room BHV-1 BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scalehouse Sample Plant (OBS) Front Gate AF-Barrel Dump Station AF Circuit -South AF Circuit-North North Control # 1 North Control# 2 CaF2 Barrel Dump Station - Operator Station KF Barrel Dump Station Date Issued 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 3/27/2014 Ambient Total Days Dose Badge at Equivalen mRem I Date Returned WMM t hour 6/27/2014 92 35.3 0.02 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 6/27/2014 92 92 92 92 92 92 2 92 92 92 92 92 92 92 2 92 2 9-2 92 92 92 92 92 92 92 92 '2 2 92 92 '92 92 92 '92 92 92 2 92 92 92 92 51.4 31.1 508.1 116.7 0 165.2 359.9 0 86.9 117.4 379.9 93.9 179.6 37.7 30.8 33.6 32 37.2 354.4 63 .1 82.5 49.7 40.9 92.8 0 0 138.7 66.1 110.1 48.7 389.1 217 260.7 218.7 0 0 0 38.7 31.2 0 271.6 0.02 0.01 0.23 0.05 0.00 0.07 0.16 0.00 0.04 0.05 0.17 0.04 0.08 0.02 0.01 0.02 0.01 0.02 0.16 0.03 0.04 0.02 0.02 0.04 0.00 0.00 0.06 0.03 0.05 0.02 0.18 0.10 0.12 0.10 0.00 0.00 0.00 0.02 0.01 0.00 0.12 mRem/ Day 0.384 0.559 0.338 5.523 1.268 0.000 1.796 3.912 0.000 0.945 1.276 4.129 1.021 1.952 0.410 0.335 0.365 0.348 0.404 3.852 0.686 0.897 0.540 0.445 1.009 0.000 0.000 1.508 0.718 1.197 0.529 4.229 2.359 2.834 2.377 0.000 0.000 0.000 0.421 0.339 0.000 2.952 mRem/ Week 2.69 3.91 2.37 38.66 8.88 0.00 12.57 27.38 0.00 6.61 8.93 28.91 7.14 13.67 2.87 2.34 2.56 2.43 2.83 26.97 4.80 6.28 3.78 3.11 7.06 0.00 0.00 10.55 5.03 8.38 3.71 29.61 16.51 19.84 16.64 0.00 0.00 0.00 2.94 2.37 0.00 20.67 ATTACHMENT F VEGETATION GRAPHS, DATA TABLE, LABORATORY RESULTS AND QAJQC (Log Scale) ...... ...... ...... ...... 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 co -...1 0) 01 .j:>. w 1\) 8/27/1981 8/27/1982 . 8/27/1983 . 8/27/1984 - 8/27/1985 8/27/1986 . 8/27/1987 8/27/1988 JJ 8/27/1989 . D) I N 8/27/1990 . N 0) 8/27/1991 . 0 0 8/27/1992 ::::J (") CD 8/27/1993 ::::J -""t 8/27/1994 D) -t a· 8/27/1995 ::::J t/1 z 8/27/1996 ::::J m < 8/27/1997 . CD T <C 8/27/1998 CD -D) -z 8/27/1999 . a· :;! ::::J 8/27/2000 -t c 0 8/27/2001 . =:::.: UJ 8/27/2002 . " :;! <C -8/27/2003 8/27/2004 . 8/27/2005 8/27/2006 . 8/27/2007 . 8/27/2008 - 8/27/2009 . 8/27/2010 - 8/27/2011 •. 8/27/2012 8/27/2013 - (Log Scale) ...... ...... ...... ...... ...... 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 co --.I 0) U1 ~ c.v 1\:) 8/27/1981 8/27/1982 8/27/1983 8/27/1984 8/27/1985 8/27/1986 8/27/1987 8/27/1988 "0 8/27/1989 C" I 8/27/1990 . N ...... 0 8/27/1991 . (") 0 8/27/1992 ::::J (') (I) 8/27/1993 ::::J -'"' 8/27/1994 I» -s· t 8/27/1995 ::::J 0 z 8/27/1996 -:; m < 8/27/1997 -(I) f (Q 8/27/1998 (I) -I» -z 8/27/1999 -s· :E ::::J 8/27/2000 -t c 8/27/2001 (") :::::: (J) "' :E 8/27/2002 . (Q --8/27/2003 8/27/2004 8/27/2005 . 8/27/2006 8/27/2007 8/27/2008 8/27/2009 8/27/2010 8/27/2011 8/27/2012 8/27/2013 WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHEAST OF MILL SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd'82 15-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nov-82 2nd '83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd'84 28-Jun-84 4th '84 14-Nov-84 2nd'85 27-Mar-85 3rd '85 15-Jul-85 4th '85 09-0ct-85 2nd '86 24-Mar-86 3rd '86 10-Jul-86 4th '86 18-Dec-86 2nd '87 20-Apr-87 3rd'87 05-Jun-87 4th '87 22-Dec-87 2nd'88 19-Apr-88 3rd '88 28-Jul-88 2nd'89 07-Apr-89 3rd '89 06-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd'90 20-Jun-90 3rd '90 17-0ct-90 1st '91 10-Apr-91 2nd '91 11-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 10-Jun-92 3rd'92 10-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd'93 12-0ct-93 1st '94 11-May-94 2nd'94 19-Jul-94 3rd'94 28-Nov-94 1st '95 11-Apr-95 2nd'95 06-Jul-95 3rd '95 15-Nov-95 1st '96 23-Apr-96 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd '97 05-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 05-Nov-98 2nd '99 15-Apr-99 3rd'99 07-Jul-99 4th '99 02-Dec-99 2nd'OO 21-Apr-00 2nd'OO 22-Jun-00 Ra-226 Ra-226 VALUE (uCi/Kg) ERROR (uCi/Kg) 3.90E-04 1.00E-05 1.40E-04 1.00E-05 1.31E-04 1.30E-05 1.60E-04 l.OOE-05 2.67E-06 1.07E-06 9.36E-05 6.20E-06 1.12E-04 1.20E-05 1.09E-04 8.00E-06 3.47E-04 1.20E-05 5.61E-04 1.99E-04 1.05E-03 3.00E-05 8.20E-05 7.00E-06 1.15E-04 l.OOE-05 5.72E-04 2.10E-05 5.01E-04 1.30E-05 8.70E-04 5.00E-05 5.90E-04 7.00E-05 1.60E-04 3.00E-05 2.10E-04 4.00E-05 4.50E-04 7.00E-05 3.20E-05 2.20E-05 5.60E-04 4.00E-05 1.50E-04 2.00E-05 6.00E-04 5.00E-05 2.60E-04 3.00E-05 1.80E-04 2.00E-05 1.60E-04 2.00E-05 1.20E-04 2.00E-05 9.10E-05 1.60E-05 4.50E-04 4.00E-05 3.60E-05 1.00E-05 l.OOE-05 7.00E-06 7.90E-05 3.50E-05 3.70E-05 2.20E-05 3.00E-05 1.50E-05 6.60E-05 2.70E-05 1.80E-04 4.00E-05 1.71E-05 1.20E-06 2.40E-04 1.50E-05 6.70E-05 5.40E-06 1.50E-05 1.50E-06 5.50E-05 5.00E-06 5.20E-05 2.50E-06 3.00E-05 2.50E-06 l.lOE-05 4.70E-07 l.lOE-05 4.30E-07 8.00E-06 1.20E-06 <9.10E-05 9.10E-05 1.80E-05 1.20E-06 5.70E-05 1.00E-06 2.00E-04 3.00E-06 6.03E-05 1.40E-06 2.30E-05 l.OOE-06 1.50E-04 3.00E-06 1.20E-06 l.OOE-07 LLD Pb-210 Pb-210 LLD uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (l.OE-06) 5.00E-08 1.10E-03 l.OOE-04 l.OOE-06 S.OOE-08 6.80E-04 8.00E-05 l.OOE-06 l.OOE-06 4.90E-04 7.00E-05 8.00E-05 5.00E-08 8.00E-04 1.70E-04 1.00E-07 l.OOE-06 1.08E-04 9.00E-06 l.OOE-05 8.00E-09 .4.97E-04 9.30E-05 l.OOE-04 6.00E-06 1.84E-04 1.20E-05 l.OOE-06 4.00E-06 7.80E-04 6.20E-05 6.00E-05 2.00E-09 3.75E-03 1.60E-04 4.00E-08 2.00E-07 7.82E-03 3.30E-04 7.00E-08 2.00E-06 3.22E-03 1.40E-04 2.00E-05 3.00E-06 7.70E-04 1.30E-04 2.00E-04 3.00E-06 5.10E-04 3.00E-05 2.00E-05 4.00E-06 2.49E-03 l.OOE-04 l.OOE-05 3.00E-06 1.57E-03 1.70E-03 2.00E-04 3.00E-06 6.80E-04 3.00E-05 3.00E-06 5.00E-08 1.50E-03 l.OOE-04 l.OOE-06 5.00E-08 9.50E-04 4.00E-05 1.00E-06 5.00E-08 1.70E-03 l.OOE-04 l.OOE-06 5.00E-08 1.40E-03 l.OOE-04 l.OOE-06 5.00E-08 1.50E-04 4.40E-04 l.OOE-06 *** 1.10E-03 1.00E-01 *** *** 2.30E-04 2.00E-05 *** 7.00E-06 2.04E-03 7.00E-05 1.40E-05 4.00E-06 3.30E-04 2.00E-05 2.20E-05 5.00E-08 3.20E-04 2.00E-05 l.OOE-06 5.00E-08 3.30E-04 2.00E-05 l.OOE-06 5.00E-06 3.00E-04 2.00E-05 l.OOE-06 2.00E-07 1.90E-04 2.00E-05 2.00E-07 5.00E-08 1.09E-03 5.00E-05 l.OOE-06 2.00E-06 l.50E-04 2.00E-05 l.OOE-05 2.00E-07 7.50E-05 2.00E-05 l.OOE-06 3.00E-06 7.10E-04 7.00E-05 2.00E-05 3.00E-06 2.80E-04 3.00E-05 2.00E-05 3.00E-06 4.30E-05 3.50E-05 2.00E-05 3.00E-06 5.30E-04 6.00E-05 2.00E-05 3.00E-05 4.40E-04 6.00E-05 2.00E-04 9.00E-08 3.00E-05 6.10E-06 4.45E-06 1.70E-07 1.70E-04 1.10E-05 8.30E-07 1.60E-07 1.40E-04 1.30E-05 7.90E-07 1.50E-07 5.10E-05 4.50E-06 7.60E-07 1.80E-07 6.70E-05 1.00E-05 8.80E-07 1.50E-07 3.20E-05 4.50E-06 1.80E-07 1.80E-07 1.40E-04 7.10E-06 9.30E-07 1.21E-07 4.10E-05 3.60E-06 6.10E-07 1.33E-07 2.10E-05 7.30E-07 6.66E-07 5.60E-07 1.40E-04 4.60E-06 1.10E-07 9.10E-05 <4.50E-04 4.50E-04 4.50E-04 6.30E-08 4.00E-05 1.80E-06 3.20E-07 8.20E-08 8.70E-05 5.00E-06 4.10E-07 1.20E-07 3.00E-04 l.OOE-05 6.00E-05 8.30E-08 1.40E-04 4.70E-06 4.20E-07 2.30E-07 2.10E-05 l.OOE-06 1.10E-06 1.20E-07 1.60E-04 8.00E-06 5.90E-07 2.80E-07 1.60E-04 l.OOE-05 1.40E-06 4th '00 21-Dec-00 1.60E-06 l.lOE-06 3.70E-07 5.10E-05 5.00E-06 1.90E-06 1st '01 30-Apr-01 l.OOE-06 l.OOE-07 2.40E-07 <1.2E-06 l.OOE-07 2.40E-07 2nd '01 14-Jun-01 2.30E-06 2.00E-07 9.90E-08 3.80E-06 2.00E-07 5.00E-07 4th '01 17-Dec-01 9.10E-06 2.40E-06 1.20E-07 3.57E-05 2.97E-06 6.00E-07 1st '02 07-May-02 3.30E-05 1.80E-06 7.60E-07 4.50E-05 2.61E-06 l.OOE-05 2nd '02 07-Jul-02 5.55E-05 2.81E-06 7.60E-07 5.31E-05 3.90E-06 l.OOE-05 4th '02 15-Dec-02 7.75E-05 3.60E-06 7.60E-07 1.29E-04 6.15E-06 l.OOE-05 1st '03 21-Mar-03 9.10E-06 1.30E-06 3.60E-07 1.13E-05 1.61E-06 3.36E-06 2nd'03 10-Jun-03 2.50E-05 1.30E-06 3.60E-07 3.26E-06 2.00E-06 7.38E-08 4th '03 20-Nov-03 5.70E-05 3.50E-06 1.50E-07 4.05E-05 5.82E-06 8.30E-07 1st '04 08-Apr-04 9.38E-05 3.70E-06 l.lOE-07 5.88E-05 3.00E-06 5.50E-07 2nd '04 12-Jun-04 5.63E-05 3.40E-06 1.80E-07 6.42E-05 5.90E-06 9.00E-07 4th '04 30-Nov-04 8.41E-05 5.50E-06 2.00E-08 2.48E-04 1.40E-05 3.00E-07 1st 'OS 21-Apr-05 S.60E-OS 3.00E-06 1.40E-07 5.80E-05 4.00E-06 6.90E-07 2nd'OS 13-Jun-OS 9.10E-06 1.50E-06 1.80E-07 1.10E-05 1.20E-OS 9.00E-07 4th 'OS 10-Nov-OS 6.00E-OS 3.00E-06 l.lOE-10 1.70E-06 6.40E-07 S.SOE-10 1st '06 03-Apr-06 8.00E-05 S.OOE-06 5.00E-08 3.40E-04 1.20E-05 1.00E-06 2nd '06 16-Jun-06 4.10E-05 3.10E-06 5.00E-08 1.16E-04 6.10E-06 1.00E-06 4th '06 28-Nov-06 1.17E-04 4.60E-06 1.90E-07 3.28E-04 9.50E-06 9.50E-07 1st '07 30-Mar-07 9.70E-OS 4.40E-06 1.90E-07 3.40E-04 8.70E-06 8.4-07 2nd '07 1-Jun-07 1.30E-05 1.60E-06 1.90E-07 1.20E-04 6.60E-06 9.70E-07 4th '07 23-Nov-07 7.00E-05 8.20E-06 2.00E-07 5.00E-04 2.00E-05 1.20E-06 1st '08 22-Apr-08 3.60E-06 3.00E-06 5.20E-07 2.30E-04 1.40E-05 1.00E-06 2nd'08 18-Jun-08 3.20E-05 3.20E-06 1.80E-06 6.90E-OS 3.50E-OS S.SOE-OS 4th '08 12-Dec-08 l.SOE-04 5.20E-06 9.90E-07 3.60E-04 2.90E-OS 3.90E-OS 1st '09 28-Apr-09 S.90E-04 1.3SE-OS l.SOE-06 3.40E-04 1.30E-OS l.SOE-06 2nd '09 17-Jun-09 1.90E-05 1.4SE-06 4.90E-07 3.60E-OS l.lOE-OS 1.80E-OS 4th '09 18-Dec-09 1.70E-04 5.90E-06 4.80E-04 1.20E-05 1st '10 13-May-10 2.20E-04 7.20E-06 1.10E-06 1.90E-04 1.90E-05 2.90E-OS 2nd '10 18-Jun-10 6.SOE-05 3.40E-06 7.60E-07 1.40E-04 1.90E-05 2.90E-05 4th '10 20-Dec-10 2.30E-05 1.70E-06 5.20E-07 l.OOE-05 1.50E-06 2.30E-06 2nd '11 23-Jun-11 2.40E-07 1.40E-07 1.80E-07 <2.9E-06 1.70E-06 2.90E-06 3rd '11 27-Jul-11 4.90E-06 6.30E-07 3.20E-07 9.50E-05 2.10E-06 2.50E-06 4th '11 23-Nov-11 7.20E-06 7.50E-07 2.90E-07 8.80E-08 4.30E-07 7.20E-07 2nd'12 11-Apr-12 4.40E-05 1.90E-06 3.60E-07 2.10E-04 2.00E-06 l.OOE-06 3rd '12 11-Jun-12 2.20E-05 8.40E-07 1.10E-07 1.30E-04 7.60E-06 5.90E-06 4th '12 06-Nov-12 3.10E-05 4.82E-07 4.63E-08 4.26E-04 3.72E-06 6.52E-07 2nd '13 30-Apr-13 1.14E-04 1.74E-06 5.34E-07 2.6SE-04 4.41E-06 5.37E-06 3rd '13 20-Jun-13 8.91E-05 2.16E-06 1.42E-06 1.42E-04 3.68E-06 6.17E-06 4th '13 14-Nov-13 1.37E-04 3.87E-06 4.71E-06 5.33E-04 1.45E-05 2.27E-05 2nd '14 16-Apr-14 9.90E-05 1.01E-06 3.91E-07 1.99E-04 3.14E-06 3.38E-06 3rd '14 10-Jun-14 2.60E-05 8.46E-07 9.19E-07 5.60E-05 3.08E-06 7.12E-06 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected dunng th1s penod (Log Scale) _.. _.. _.. _.. 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 CXl ""-1 en 01 ~ c.u 1\) 01-Jan-81 01-Jan-82 =e ~ 01-Jan-83 =i 01-Jan-84 m 3: 01-Jan-85 m C/) 01-Jan-86 )> 3: 01-Jan-87 -r-r-01-Jan-88 I 01-Jan-89 z 0 01-Jan-90 -JJ -1 ~ 01-Jan-91 -m )> 01-Jan-92 -C/) -1 01-Jan-93 0 t ., 01-Jan-94 s: JJ 01-Jan-95 r- iJl -r-r\J f,JJ 1\J 01-Jan-96 (l) -·D) -I T 01-Jan-97 :;:ti:;N CCN -en -u 01-Jan-98 · D) 0" :::J r\J 01-Jan-99 c. ~ 0 "tt 01-Jan-00 · C" I 01-Jan-01 1\) ...... 0 01-Jan-02 0 0 01-Jan-03 :::J (') 01-Jan-04 ' CD :::J -.., 01-Jan-05 D) -s· 01-Jan-06 :::J en 01-Jan-07 --· :::J 01-Jan-08 < CD 01-Jan-09 cg ! 01-Jan-10 " D) -s· 01-Jan-11 :::J 01-Jan-12 01-Jan-13 01-Jan-14 WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHWEST OF MILL SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd'82 15-Apr-82 3rd'82 01-Jul-82 4th '82 30-Nov-82 2nd'83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd'84 28-Jun-84 4th '84 14-Nov-84 2nd '85 27-Mar-85 3rd '85 15-Jul-85 4th '85 09-0ct-85 2nd '86 24-Mar-86 3rd'86 10-Jul-86 4th '86 18-Dec-86 2nd'87 20-Apr-87 3rd'87 05-Jun-87 4th '87 22-Dec-87 2nd'88 19-Apr-88 3rd '88 28-Jul-88 2nd'89 07-Apr-89 3rd'89 06-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd '90 20-Jun-90 3rd '90 17-0ct-90 1st '91 10-Apr-91 2nd '91 11-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 10-Jun-92 3rd '92 10-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd'93 12-0ct-93 1st '94 11-May-94 2nd'94 19-Jul-94 3rd'94 28-Nov-94 1st '95 11-Apr-95 2nd'95 06-Jul-95 3rd '95 15-Nov-95 1st '96 23-Apr-96 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd '97 05-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 05-Nov-98 2nd '99 15-Apr-99 3rd '99 07-Jul-99 4th '99 02-Dec-99 2nd '00 21-Apr-00 Ra-226 VALUE (uCi/Kg) 2.73E-03 2.00E-04 1.04E-04 2.00E-05 2.36E-06 8.58E-05 1.19E-04 9.78E-05 2.08E-04 6.05E-04 1.10E-04 6.10E-05 1.07E-04 8.86E-04 6.66E-04 5.20E-04 4.10E-04 1.60E-04 3.60E-04 2.60E-04 3.10E-05 6.20E-04 3.40E-04 5.10E-04 3.60E-04 1.70E-04 8.80E-05 3.00E-04 3.10E-04 5.00E-04 2.00E-05 6.50E-06 1.20E-04 1.80E-05 5.20E-05 5.10E-05 1.20E-04 3.73E-05 2.40E-04 8.40E-05 1.90E-05 1.20E-04 8.30E-05 3.60E-05 3.30E-05 5.40E-06 8.90E-06 <9.20E-05 < 6.50E-08 4.20E-05 6.20E-05 5.45E-05 l.lOE-04 3.70E-05 Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (1.0E-06) S.OOE-05 5.00E-08 7.10E-03 3.00E-04 1.00E-06 l.OOE-05 5.00E-08 8.30E-04 5.00E-05 1.00E-06 9.00E-06 7.00E-06 6.40E-04 5.00E-05 4.00E-05 l.OOE-05 5.00E-08 2.20E-04 9.00E-05 l.OOE-07 9.50E-07 1.00E-06 8.00E-05 l.OOE-05 l.OOE-05 1.36E-05 2.00E-08 3.53E-04 1.90E-05 l.OOE-05 l.lOE-05 5.00E-06 1.58E-04 1.30E-05 l.OOE-05 7.00E-06 2.00E-06 2.16E-03 3.40E-04 3.00E-04 l.OOE-05 3.00E-09 1.60E-03 7.00E-05 3.00E-08 1.64E-04 2.00E-07 2.58E-03 l.lOE-04 3.00E-08 8.00E-06 3.00E-06 8.63E-04 4.20E-05 3.00E-05 6.00E-06 2.00E-06 5.40E-04 5.00E-05 5.00E-05 6.00E-06 2.00E-06 3.80E-04 3.00E-05 2.00E-05 1.80E-05 2.00E-06 4.40E-03 1.90E-04 3.00E-05 1.80E-05 3.00E-06 4.78E-03 2.10E-04 6.00E-05 l.OOE-04 3.00E-06 1.70E-03 l.OOE-04 6.00E-05 l.OOE-04 5.00E-08 1.60E-03 l.OOE-04 l.OOE-06 3.00E-05 5.00E-08 5.50E-04 4.00E-05 l.OOE-06 5.00E-05 5.00E-08 1.80E-03 l.OOE-04 l.OOE-06 5.00E-05 5.00E-08 1.90E-03 l.OOE-04 l.OOE-06 1.90E-05 5.00E-08 1.60E-04 4.00E-05 l.OOE-06 5.00E-05 *** 1.70E-03 l.OOE-04 *** 3.00E-05 *** 7.40E-04 3.00E-05 *** 6.00E-05 7.00E-06 1.00E-03 7.00E-05 1.40E-05 3.00E-05 4.00E-06 4.80E-04 2.00E-05 2.20E-05 2.00E-05 5.00E-08 3.20E-04 2.00E-05 1.00E-06 1.60E-05 5.00E-08 2.90E-04 2.00E-05 1.00E-06 3.00E-05 5.00E-06 4.10E-04 2.00E-05 l.OOE-06 3.00E-05 2.00E-07 4.70E-04 2.00E-05 2.00E-07 4.00E-05 5.00E-08 1.50E-03 l.OOE-04 l.OOE-06 8.00E-06 2.00E-06 9.60E-05 1.40E-05 l.OOE-05 6.00E-06 2.00E-06 1.20E-04 2.00E-05 l.OOE-06 4.00E-05 3.00E-06 1.21E-03 8.00E-05 2.00E-05 1.70E-05 3.00E-06 2.10E-04 3.00E-05 2.00E-05 1.90E-05 3.00E-06 1.70E-05 3.60E-05 2.00E-05 2.30E-05 3.00E-06 7.10E-04 6.00E-05 2.00E-05 l.OOE-05 3.00E-05 9.80E-04 1.60E-04 2.00E-04 1.60E-06 8.40E-08 7.80E-05 7.10E-06 4.20E-07 1.50E-05 1.70E-07 2.60E-04 1.30E-05 8.30E-07 6.10E-06 1.50E-07 1.20E-04 1.10E-05 7.50E-05 1.50E-06 1.40E-07 4.50E-05 4.30E-06 7.20E-07 6.80E-06 1.40E-07 l.OOE-05 5.80E-06 7.10E-07 3.30E-06 1.90E-07 6.80E-05 6.30E-06 1.80E-07 2.50E-06 1.60E-07 8.50E-05 5.60E-06 8.40E-07 2.30E-06 1.70E-07 4.40E-05 4.80E-06 8.40E-07 3.50E-07 1.56E-07 3.20E-05 9.00E-07 7.83E-07 7.20E-07 5.40E-07 3.40E-04 6.70E-06 l.lOE-07 9.20E-05 9.20E-05 <4.60E-04 4.60E-04 4.60E-04 6.50E-08 6.50E-08 <3.20E-07 3.20E-07 3.20E-07 l.OOE-06 l.lOE-07 1.70E-04 l.OOE-05 5.50E-07 l.OOE-06 l.OOE-07 1.40E-04 7.00E-06 1.00E-07 1.40E-06 8.30E-08 '9.20E-05 4.00E-06 4.20E-07 3.00E-06 2.20E-07 2.80E-05 l.OOE-06 l.lOE-06 l.OOE-06 2.40E-07 2.70E-04 l.OOE-05 1.20E-06 2nd '00 22-Jun-00 2.90E-05 l.OOE-06 3.30E-07 2.80E-04 2.00E-05 1.70E-06 4th '00 21-Dec-00 2.30E-06 1.40E-06 3.70E-07 3.30E-04 S.OOE-05 1.90E-06 1st '01 30-Apr-01 2.10E-05 1.00E-06 l.SOE-07 <7.6E-07 N/A 7.60E-07 2nd '01 14-Jun-01 1.30E-06 4.00E-08 1.20E-07 1.80E-06 3.00E-08 5.90E-07 4th '01 17-Dec-01 3.70E-05 7.67E-07 8.30E-08 6.72E-05 2.62E-06 6.00E-07 1st '02 07-May-02 4.90E-05 2.40E-06 7.60E-07 1.28E-04 5.61E-06 l.OOE-05 2nd'02 07-Jul-02 8.88E-05 4.32E-06 7.60E-07 8.33E-05 4.32E-06 l.OOE-05 4th '02 15-Dec-02 l.SOE-04 6.20E-06 7.60E-07 3.16E-04 1.07E-05 l.OOE-05 1st '03 21-Mar-03 S.OOE-05 3.40E-06 2.71E-06 <4.2e-6 4.20E-06 2nd'03 10-Jun-03 5.60E-05 2.00E-06 4.10E-07 1.88E-04 5.14E-06 8.20E-08 4th '03 20-Nov-03 3.20E-04 8.20E-06 1.70E-07 4.89E-04 1.25E-05 8.30E-07 1st '04 08-Apr-04 6.29E-05 4.10E-06 2.00E-07 1.94E-05 4.00E-06 l.OOE-06 2nd'04 12-Jun-04 6.51E-05 3.40E-06 1.30E-07 1.87E-05 3.90E-06 6.SOE-07 4th '04 30-Nov-04 7.50E-05 4.60E-06 2.00E-08 4.45E-04 1.40E-05 3.00E-07 1st 'OS 21-Apr-05 4.90E-05 2.70E-06 1.30E-07 1.27E-04 4.80E-06 6.SOE-07 2nd'OS 13-Jun-05 2.30E-05 2.10E-06 l.SOE-07 4.70E-05 5.10E-06 7.60E-07 4th 'OS 10-Nov-05 7.40E-05 3.SOE-06 1.20E-10 2.40E-06 8.10E-08 5.80E-10 1st '06 03-Apr-06 1.00E-04 6.00E-06 S.OOE-08 6.54E-04 l.SOE-05 l.OOE-06 2nd '06 16-Jun-06 9.50E-05 5.90E-06 S.OOE-08 4.48E-04 1.40E-05 1.00E-06 4th '06 28-Nov-06 8.13E-05 4.10E-06 2.20E-07 3.25E-04 1.12E-06 1.00E-05 1st '07 30-Mar-07 4.30E-05 2.60E-06 1.70E-07 2.64E-04 7.20E-06 8.60E-07 2nd '07 1-Jun-07 5.10E-05 3.20E-06 2.30E-07 5.30E-04 1.40E-06 1.20E-06 4th '07 23-Nov-07 7.30E-05 6.60E-06 S.OOE-08 7.00E-04 2.20E-05 1.10E-06 1st '08 22-Apr-08 2.80E-06 2.80E-06 7.20E-07 4.40E-04 2.00E-05 l.OOE-06 2nd '08 18-Jun-08 3.20E-06 3.30E-06 1.80E-06 1.40E-04 3.30E-05 S.SOE-05 4th '08 12-Dec-08 7.30E-05 3.20E-06 7.40E-07 4.40E-04 2.50E-05 3.20E-05 1st '09 28-Apr-09 5.25E-05 3.60E-06 l.lOE-06 1.90E-04 l.SOE-05 2.20E-05 2nd '09 17-Jun-09 2.30E-05 1.60E-05 5.20E-07 4.30E-05 l.OOE-05 1.70E-05 4th '09 18-Dec-09 S.SOE-05 3.50E-06 3.00E-04 1.10E-05 1st '10 13-May-10 1.90E-04 6.10E-06 9.40E-07 5.10E-04 2.40E-05 3.10E-05 2nd '10 18-Jun-10 2.30E-05 2.00E-06 7.70E-07 8.30E-05 1.80E-05 2.90E-05 4th '10 20-Dec-10 8.60E-06 9.10E-07 3.90E-07 l.lOE-07 6.80E-07 1.10E-06 2nd '11 23-Jun-11 2.10E-07 1.20E-07 1.40E-07 <2.2E-06 1.30E-06 2.20E-06 3rd '11 28-Jul-11 4.20E-06 5.40E-07 2.70E-07 2.30E-04 2.SOE-06 2.30E-06 4th '11 23-Nov-11 7.70E-06 6.80E-07 2.30E-07 <5.8E-08 3.40E-07 5.80E-07 2nd'12 11-Apr-12 l.SOE-05 9.50E-07 2.60E-07 <7.0E-07 6.00E-07 l.OOE-06 3rd '12 11-Jun-12 8.30E-06 5.40E-07 1.20E-07 1.40E-04 8.30E-06 6.SOE-06 4th '12 06-Nov-12 2.34E-05 4.10E-07 7.71E-08 4.59E-04 3.83E-06 6.18E-07 2nd'13 30-Apr-13 9.04E-05 1.68E-06 8.58E-07 2.24E-04 4.46E-06 4.68E-06 3rd '13 20-Jun-13 2.58E-06 9.59E-07 8.06E-07 1.06E-04 2.30E-06 3.28E-06 4th '13 14-Nov-13 1.43E-04 3.70E-06 2.17E-06 4.65E-04 1.17E-05 1.80E-05 2nd'14 16-Apr-14 2.53E-05 6.29E-07 5.51E-07 5.70E-05 2.21E-06 4.52E-06 3rd '14 10-Jun-14 2.53E-05 S.SSE-07 5.77E-07 7.68E-05 2.08E-06 3.66E-06 *2nd quarter of 1996 San Juan County, Utah, was declared a d1saster area due to drought, no samples were collected dunng th1s penod 0 0 0 0 0 0 m m m I I I 0 0 0 co ..._. O'l 01-Jan-81 01-Jan-82 01-Jan-83 01-Jan-84 - 01-Jan-85 01-Jan-86 01 -Jan-87 01-Jan-88 01-Jan-89 _, 01-Jan-90 01-Jan-91 01-Jan-92 •· t 01-Jan-93 01 -Jan-94 JJ "' 01-Jan-95 N 1\) (j) 01-Jan-96 T 01-Jan-97 -u 01-Jan-98 • 0" ~ 01-Jan-99 -0 01-Jan-00 01 -Jan-01 - 01-Jan-02 01-Jan-03 - 01-Jan-04 - 01-Jan-05 - 01-Jan-06 01-Jan-07 - 01 -Jan-08 01-Jan-09 01-Jan-1 0 01-Jan-11 01-Jan-12 01-Jan-13 01-Jan-14 (Log Scale) ...... 0 0 m I 0 01 0 0 m I 0 ~ ...... 0 0 m I 0 w 0 0 m I 0 1\) :E ::I: =t m s:: m en l> s:: r r z 0 ::tl -4 ::I: :E m en -4 0 "TI 3: r -· f>::t~ -·I» -. "'I\) CCN -0) I» :::::s c. "'tJ C" N ...... 0 0 0 :::::s (') C'D :::::s -a a· :::::s U) 5' ~ (Q C'D -I» -a· :::::s WHITE MESA MILL FORAGE RADIONUCLIDE DATA SOUTHWEST OF MILL SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd '82 15-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nov-82 2nd '83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-84 2nd '85 27-Mar-85 3rd '85 15-Jul-85 4th '85 09-0ct-85 2nd'86 24-Mar-86 3rd '86 10-Jul-86 4th '86 18-Dec-86 2nd'87 20-Apr-87 3rd '87 05-Jun-87 4th '87 22-Dec-87 2nd '88 19-Apr-88 3rd '88 28-Jul-88 2nd '89 07-Apr-89 3rd'89 06-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd'90 20-Jun-90 3rd '90 17-0ct-90 1st '91 10-Apr-91 2nd'91 11-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 10-Jun-92 3rd'92 10-Jun-92 1st '93 13-Apr-93 2nd'93 26-Jun-93 3rd'93 12-0ct-93 1st '94 11-May-94 2nd'94 19-Jul-94 3rd'94 28-Nov-94 1st '95 11-Apr-95 2nd '95 06-Jul-95 3rd '95 15-Nov-95 1st '96 23-Apr-96 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 1st'97 21-Apr-97 3rd'97 05-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd'98 16-Jun-98 4th '98 05-Nov-98 2nd '99 15-Apr-99 3rd '99 07-Jul-99 4th '99 02-Dec-99 2nd'OO 21-Apr-00 Ra-226 VALUE (uCi/Kg) 9.50E-04 3.00E-05 1.37E-05 3.40E-04 1.75E-05 7.13E-04 5.39E-05 6.40E-05 8.27E-05 2.72E-04 4.73E-04 6.60E-05 2.83E-04 1.57E-04 3.78E-04 2.60E-04 4.10E-04 2.90E-04 1.80E-04 2.30E-04 1.50E-04 3.10E-04 1.30E-04 4.30E-04 2.50E-04 l.lOE-04 6.10E-05 3.40E-05 B.OOE-05 6.50E-05 1.60E-05 1.90E-05 1.60E-05 2.60E-05 3.00E-05 3.10E-05 2.00E-05 1.75E-05 l.OOE-04 1.70E-05 6.40E-06 2.30E-05 4.20E-05 2.10E-05 5.50E-06 5.30E-06 2.50E-05 <7.90E-05 3.60E-07 4.30E-05 2.40E-05 2.23E-05 1.50E-04 l.OOE-04 Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCl/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCI/Kg (l.OE-06) 2.00E-05 5.00E-08 1.50E-04 l.OOE-05 l.OOE-06 3.00E-06 5.00E-08 1.50E-04 2.00E-05 l.OOE-06 3.00E-06 3.00E-06 3.80E-04 4.00E-05 4.00E-05 2.00E-05 5.00E-08 3.68E-03 2.70E-04 l.OOE-07 3.00E-06 2.00E-06 7.92E-04 4.00E-06 2.00E-05 7.30E-05 9.00E-08 2.51E-03 3.00E-04 3.00E-04 4.50E-06 2.00E-06 6.88E-04 4.30E-05 4.00E-05 7.00E-06 4.00E-06 1.20E-03 l.OOE-04 4.00E-05 6.30E-06 3.00E-09 1.80E-03 l.OOE-04 9.00E-08 1.48E-04 2.00E-07 4.70E-03 7.20E-04 3.00E-07 1.60E-07 3.00E-06 7.07E-04 3.60E-05 3.00E-05 7.00E-06 4.00E-06 4.90E-04 3.00E-05 3.00E-05 2.00E-05 7.00E-06 1.50E-03 l.OOE-04 7.00E-05 1.00E-05 4.00E-06 4.14E-03 1.80E-04 3.00E-05 l.OOE-05 2.00E-06 1.65E-02 7.00E-04 l.OOE-04 2.00E-05 2.00E-06 1.70E-03 1.00E-04 l.OOE-04 7.00E-05 5.00E-08 2.20E-03 l.OOE-04 1.00E-06 4.00E-05 5.00E-08 7.50E-04 5.00E-05 l.OOE-06 3.00E-05 5.00E-08 2.40E-03 1.00E-04 l.OOE-06 5.00E-05 5.00E-08 2.90E-03 1.00E-04 l.OOE-06 3.00E-05 5.00E-08 4.30E-03 2.00E-04 1.00E-06 4.00E-05 *** 4.20E-03 l.OOE-04 *** 2.00E-05 *** 1.50E-03 l.OOE-04 *** 5.00E-05 1.40E-05 3.50E-03 1.40E-04 2.70E-05 3.00E-05 5.00E-06 2.39E-03 5.00E-05 2.50E-05 2.00E-05 5.00E-08 6.60E-04 3.00E-05 l.OOE-06 1.40E-05 5.00E-08 6.10E-04 3.00E-05 1.00E-06 1.10E-05 5.00E-06 2.20E-04 l.OOE-05 l.OOE-06 6.00E-06 2.00E-07 1.20E-04 l.OOE-05 2.00E-07 1.40E-05 5.00E-08 9.10E-04 5.00E-05 l.OOE-06 7.00E-06 2.00E-06 3.20E-04 2.00E-05 l.OOE-05 l.OOE-05 2.00E-07 2.20E-04 2.00E-05 1.00E-06 1.80E-05 3.00E-06 7.60E-04 6.00E-05 2.00E-05 2.00E-05 3.00E-06 3.40E-04 3.00E-05 2.00E-05 1.40E-05 3.00E-06 O.OOE+OO 3.00E-05 2.00E-05 1.60E-05 3.00E-06 4.20E-04 6.00E-05 2.00E-05 5.00E-06 3.00E-05 3.90E-04 8.00E-05 2.00E-04 1.70E-06 7.60E-08 1.30E-04 7.80E-06 3.80E-07 9.00E-06 1.50E-07 2.60E-04 1.20E-05 7.40E-07 1.50E-06 1.60E-07 1.60E-04 1.50E-05 8.10E-07 6.00E-07 1.40E-07 4.40E-05 4.20E-06 7.00E-07 2.20E-06 1.70E-07 6.60E-05 9.60E-06 8.30E-07 2.20E-06 1.70E-07 l.OOE-04 6.70E-06 1.80E-07 2.00E-06 1.60E-07 1.90E-04 7.30E-06 8.20E-07 4.20E-07 1.40E-07 3.30E-05 3.90E-06 7.00E-07 3.20E-07 1.26E-07 1.90E-05 6.90E-07 6.34E-07 9.50E-07 5.90E-07 1.30E-04 4.70E-06 1.20E-07 7.90E-05 7.90E-05 <3.90E-04 3.90E-04 3.90E-04 1.40E-07 3.30E-08 <1.7E-07 1.70E-07 1.70E-07 1.00E-06 7.60E-08 2.50E-04 l.OOE-05 3.80E-07 l.OOE-06 1.20E-07 1.70E-04 8.00E-06 6.20E-07 8.60E-07 1.20E-07 2.30E-04 7.00E-06 5.90E-07 3.00E-06 2.00E-07 1.70E-05 l.OOE-06 l.OOE-06 2.00E-06 1.20E-07 1.10E-04 7.00E-06 6.10E-07 2nd'OO 22-Jun-00 1.30E-06 1.00E-07 2.40E-07 2.00E-04 l.OOE-05 1.20E-06 4th '00 21-Dec-00 1.20E-06 9.00E-07 2.40E-07 1.20E-04 3.00E-05 1.20E-06 1st '01 30-Apr-01 1.80E-06 1.00E-07 1.70E-07 <::8.3E-07 N/A 8.30E-07 2nd'01 14-Jun-01 2.60E-06 2.00E-07 9.90E-08 l.lOE-06 2.00E-08 5.00E-07 4th '01 17-Dec-01 2.63E-06 4.60E-05 1.20E-07 9.40E-05 3.72E-06 6.00E-07 1st '02 07-May-02 3.50E-05 2.20E-06 7.60E-07 1.36E-04 5.61E-06 1.00E-05 2nd'02 07-Jul-02 4.02E-05 2.34E-06 7.60E-07 7.04E-05 4.11E-06 1.00E-05 4th '02 15-Dec-02 8.10E-05 3.90E-06 7.60E-07 2.87E-04 8.54E-06 l.OOE-05 1st '03 21-Mar-03 3.70E-05 2.60E-06 2.41E-06 2.69E-05 2.01E-06 3.73E-06 2nd '03 10-Jun-03 1.30E-05 l.OOE-06 5.20E-07 <l.OOE-07 1.00E-07 4th '03 20-Nov-03 1.60E-04 1.30E-05 1.20E-07 1.42E-04 6.42E-06 5.90E-07 1st '04 08-Apr-04 1.40E-04 7.70E-06 l.lOE-07 6.10E-06 2.70E-06 5.50E-07 2nd'04 12-Jun-04 6.51E-05 3.20E-06 1.50E-07 5.27E-05 4.90E-06 7.60E-07 4th '04 30-Nov-04 8.40E-05 5.70E-06 3.00E-08 3.39E-04 1.60E-05 3.00E-07 1st '05 21-Apr-05 1.70E-05 1.60E-06 1.30E-07 4.50E-05 3.50E-06 6.50E-07 2nd '05 13-Jun-05 1.50E-05 1.60E-06 1.40E-07 7.00E-05 5.10E-06 6.90E-07 4th '05 10-Nov-05 3.80E-05 2.10E-06 8.60E-10 1.20E-06 4.80E-08 4.30E-10 1st '06 03-Apr-06 l.OOE-04 6.00E-06 5.00E-08 3.30E-04 l.lOE-05 l.OOE-06 2nd '06 16-Jun-06 3.40E-05 2.50E-06 5.00E-08 1.37E-04 6.00E-06 1.00E-06 4th '06 28-Nov-06 7.31E-05 3.20E-06 1.60E-07 2.98E-04 8.50E-06 8.20E-07 1st '07 30-Mar-07 3.00E-05 2.20E-06 1.70E-07 3.20E-04 7.90E-06 8.40E-07 2nd'07 1-Jun-07 l.lOE-04 4.60E-06 2.3-07 3.20E-04 1.10E-05 1.10E-06 4th '07 23-Nov-07 5.60E-05 5.20E-06 5.00E-08 6.40E-04 1.90E-05 1.00E-06 1st '08 22-Apr-08 3.20E-05 2.30E-06 7.20E-07 2.30E-04 1.50E-05 l.OOE-06 2nd '08 18-Jun-08 1.25E-05 2.20E-06 1.80E-06 5.00E-05 3.00E-05 4.80E-03 4th '08 12-Dec-08 9.20E-05 4.10E-06 9.60E-07 4.10E-04 3.00E-05 4.00E-05 1st '09 28-Apr-09 2.60E-05 2.90E-06 1.40E-06 3.70E-05 1.50E-06 2.50E-05 2nd '09 17-Jun-09 2.40E-05 1.40E-06 3.90E-07 3.50E-05 7.90E-06 1.30E-05 4th '09 18-Dec-09 3.10E-05 2.30E-06 2.10E-04 8.40E-06 1st '10 13-May-10 2.00E-05 2.10E-06 9.40E-07 5.60E-05 1.50E-05 2.40E-05 2nd '10 18-Jun-10 1.10E-05 1.30E-06 6.60E-07 7.80E-05 1.60E-05 2.50E-05 4th '10 20-Dec-10 6.70E-06 9.10E-07 4.80E-07 8.00E-07 7.90E-07 1.30E-06 2nd '11 23-Jun-11 <1.7E-07 6.90E-08 1.70E-07 <2.5E-06 1.50E-06 2.50E-06 3rd '11 27-Jul-11 1.60E-05 1.00E-06 2.60E-07 9.50E-05 1.60E-06 1.70E-06 4th '11 23-Nov-11 7.80E-07 2.50E-07 2.30E-07 <5.9E-07 3.50E-07 5.90E-07 2nd'12 11-Apr-12 5.00E-06 6.00E-07 3.00E-07 <7.0E-07 7.00E-07 l.OOE-06 3rd '12 11-Jun-12 1.90E-08 6.20E-08 l.lOE-07 <::2.5E-07 1.30E-06 2.20E-06 4th '12 06-Nov-12 1.49E-05 3.41E-07 4.25E-08 4.45E-04 4.01E-06 8.57E-07 2nd '13 30-Apr-13 4.50E-05 1.19E-06 5.39E-07 3.62E-04 6.30E-06 9.90E-06 3rd '13 20-Jun-13 1.51E-05 1.06E-06 1.96E-06 6.71E-05 2.93E-06 6.24E-06 4th '13 14-Nov-13 1.18E-04 3.39E-06 2.97E-06 5.92E-04 1.27E-05 1.62E-05 2nd'14 16-Apr-14 4.65E-05 1.08E-06 7.35E-07 2.13E-04 5.93E-06 1.31E-05 3rd'14 10-Jun-14 1.23E-05 4.97E-07 6.97E-07 2.46E-05 1.84E-06 4.63E-06 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period (Log Scale) .. .... .... .... .... - 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m m m I I I I I I I I + 0 0 0 0 0 0 0 0 0 co --.J (j) U1 .j:>. U) 1\) .... 0 01-Jan-81 :e 01-Jan-82 -::I: ::::j 01-Jan-83 -m 01-Jan-84 • s: m 01-Jan-85 en )> 01-Jan-86 s: -r- 01-Jan-87 r- I 01-Jan-88 en 0 01-Jan-89 c: -1 01-Jan-90 ::I: :e 01-Jan-91 m en 01-Jan-92 -1 0 t 01-Jan-93 "T1 01-Jan-94 s: JJ r-~ 01-Jan-95 c• 1\.) OJ:J 0) 01-Jan-96 -·D) -I T ~N 01-Jan-97 <CN -en -u 01-Jan-98 D) 0" :::s ~ Q. 0 01-Jan-99 -"'C 01-Jan-00 C" I N 01-Jan-01 ..... 0 01-Jan-02 0 0 01-Jan-03 :::s (') (I) 01-Jan-04 -:::s -""'' 01-Jan-05 • D) -a· 01-Jan-06 -:::s tn 01-Jan-07 :::s 01-Jan-08 ~ < (I) (Q 01-Jan-09 -(I) -D) 01-Jan-10 -a· 01-Jan-11 -:::s 01-Jan-12 - 01-Jan-13 01-Jan-14 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 28,2014 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Vegetation Analysis North East 347128001 SOLID 16-APR-14 12:45 21-APR-14 Client Qualifier Result Uncertainty __ ;;_ ~ad Gas Flow Proportional Counting JFPC, Pb210, Solid "As Received" ~ead-210 0.000199 +/-3.14E-06 JFPC, Total Alpha Radium, solid "As Received" 'otal Radium 9.90E-05 +/-1.01E-06 [he following Prep Methods were performed: v1ethod Description )ry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: \1ethod Description DOE RP280 Modified EPA 900.1 Modified ;urrogate/Tracer Recovery ~ead Carrier Test GFPC, Pb210, Solid "As Received" MDC 3.38E-06 3.91E-07 3arium Carrier GFPC, Total Alpha Radium, solid "As Received" 'llotes: RL 1.00E-06 5.00E-08 Analyst CXC1 ::::ounting Uncertainty is calculated at the 68% confidence level ( 1-sigma) . ........ Project: Client ID: DNMI00101 DNMI001 Units DF Analyst Date Time Batch Method uCi/kg uCilkg Date 04/22/14 Result KSD1 05/27/14 1658 1385433 KSDI 05/27/14 1553 1385421 Time Prep Batch 1410 1382146 Analyst Comme-'-n_ts'-_ Nominal Recovery% 87.3 86.5 AcceEtable Limits (25%-125%) (25%-125%) 2 GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: July 18,2014 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Vegetation Analysis North East 350589001 Vegetation 10-JUN-14 08:45 13-JUN-14 Client Qualifier Result Uncertainty -------'"-- {.ad Gas Flow Proportional Counting }FPC, Pb210, Solid "As Received" MDC "ead-21 0 5.60E-05 +/-3.08E-06 7.12E-06 }FPC, Total Alpha Radium, solid "As Received" 'otal Radium 2.60E-05 +/-8.46E-07 9.19E-07 rhe following Prep Methods were perfo_rm_e.;_d.;_: __ ~- V1ethod Description )ry . Qil Prep Dry . oil Prep GL-RAD-A-021 The following Analytical Methods were performed: \1ethod Description DOE RP280 Modified EPA 900.1 Modified ;urrogate/Tracer Recovery "ead Carrier 3arium Carrier 'llotes: Test GFPC, Pb210, Solid "As Received" GFPC, Total Alpha Radium, solid "As Received" RL \.OOE-06 5.00E-08 Analyst KYW2 =::ounting Uncertainty is calculated at the 68% confidence level (1-sigma). Project: Client ID: DNMI00101 DNMIOOI Units DF Analyst Date Time Batch Method uCi/kg uCi/kg Date 06/16/14 Result TCI 07/16/14 TCI 07/15/14 Time Prep Batch 1756 1396221 Analyst Comments Nominal Recovery~ 113 93.1 0633 1396265 1636 1396264 Acceptable Limits (25%-125%) (25%-125%) 2 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: May 28,2014 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Vegetation Analysis North West 347128002 SOLID 16-APR-14 13:15 21-APR-14 Client Qualifier Result Uncertainty ~ad Gas Flow Proportional Counting :JFPC, Pb210, Solid "As Received" MDC ,ead-2!0 5.70E-05 +/-2.2lE-06 4.52E-06 ]FPC, Total Alpha Radium, solid "As Received" ~otal Radium 2.53E-05 +/-6.29E-07 5.51E-07 rhe following Prep Methods were performed: RL l.OOE-06 5.00E-08 Vfethod De cription )ry. II Pr.cp Dry Soil Prep GL-RAD-A-021 AnalysL --c""x=c( The following Analytical Methods were performed: \tlethod Description DOE RP28-'--0 M-od-ifi-Jed EPA 900.1 Modified 'UITogate/Tracer Recovery ,ead Carrier 3arium Carrier ~otes: Test GFPC, Pb21 0, Solid "As Received" GFPC, Total Alpha Radium, solid "As Received" :ounting Uncertainty is calculated at the 68% confidence level (1-sigma). Project: Client ID: DNMI00101 DNMIOOl Units DF Analyst Date Time Batch Method ---- uCilkg uCi/kg Date 04/22/14 Result KSDl 05/27/14 1658 1385433 KSDl 05/27/14 1553 !385421 Time Prep Batch ----:1-:-4 '"""10,...-1382146 Anal st Comments Nominal Recovery% 91.5 88.3 Acceptable Limits (25%-!25%) (25%-125%) 2 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: July 18,2014 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Vegetation Analysis North West 350589002 Vegetation 10-JUN-14 08:15 13-JUN-14 Client Parameter Qualifier Result Uncertainty ~ad Gas Flow Proportional Counting }FPC, Pb210, Solid "As Received" "ead-21 0 7.68E-05 +/-2.08E-06 }FPC, Total Alpha Radium, solid "As Received" ~otal Radium 2.53E-05 +/-5.55E-07 MDC 3.66E-06 5.77E-07 rhe following Prep Methods wer:..::.e..E.p:..::.e.:..:rfi:..:o.:..:rm=.:..ed=::...._ ______ _ \1ethod Description )ry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: \1ethod De""s=-=cr~ip"-'t"-'io:..::n'------- DOE RP280 Modified EPA 900.1 Modified ;urrog~te/Tracer Recovery "ead Carrier 3arium Carrier 'Jotes: Test GFPC, Pb210, Solid "As Received" GFPC, Total Alpha Radium, solid "As Received" RL l.OOE-06 5.00E-08 Analyst KYW2 :=ounting Uncertainty is calculated at the 68% confidence level (1-sigma). Project: Client ID: DNMI00101 DNMI001 Units DF Analyst Date uCi/kg uCi/kg Date 06/16/14 Result TC1 07/16/14 TC1 07/15/14 Time Prep Batch 1756 1396221 Anal st Comments Nominal Recovery% 114 96.7 Time Batch Method 0634 1396265 1636 1396264 Acceptable Limits (25%-125%) (25%-125%) 2 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Vegetation Analysis South West 347128003 SOLID 16-APR-14 14:00 21-APR-14 Client Qualifier Result Uncertainty {ad Gas Flow Proportional Counting :JFPC, Pb21 0, Solid "As Received" MDC "ead-21 0 0.000213 +/-5.93E-06 1.31E-05 :JFPC, Total Alpha Radium, solid "As Received" 'otal Radium 4.65E-05 +/-1.08E-06 7.35E-07 rhe following Prep Methods were performed: vtethod Description )ry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: \1ethod Description DOE RP280 Modified EPA 900.1 Modified ;urr~ate/Tracer Recovery "ead Carrier 3arium Carrier 'lotes: Test GFPC, Pb210, Solid "As Received" GFPC, Total Alpha Radium, solid "As Received" RL l.OOE-06 5.00E-08 Analyst CXCI ::::ounting Uncertainty is calculated at the 68% confidence level (1-sigma). Report Date: May 28,2014 Project: Client ID: DNMI00101 DNMI001 Units OF Analyst Date Time Batch Method uCi/kg uCilkg Date 04/22/14 Result KSDl 05/27/14 1658 1385433 KSD1 05/27/14 1553 1385421 2 Time Prep Batch 1410 1382146 Analvst Comments Nominal Recovery% 88.0 78.5 Acceptable Limit~ (25%-125%) (25%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www .gel. com Certificate of Analysis Report Date: July 18,2014 Company : Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Vegetation Analysis South West 350589003 Vegetation 10-JUN-14 07:45 13-JUN-14 Client Project: Client ID: DNMI00101 DNMI001 Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method ------------------~----------~------------------------------Parameter {ad Gas Flow Proportional Counting ]FPC, Pb210, Solid "As Received" ~ead-21 0 2.46E-05 +/-1.84E-06 :JFPC, Total Alpha Radium, solid "As Received" ~ota1 Radium 1.23E-05 +/-4.97E-07 fhe following Prep Methods were performed: vtethod Description )ry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: \1ethod Description DOE RP280 Modified EPA 900.1 Modified ;urrogate/Tracer Recovery Test ~ead Carrier GFPC, Pb210, Solid "As Received" 4.63E-06 6.97E-07 ~arium Carrier GFPC, Total Alpha Radium, solid "As Received" ~otes: l.OOE-06 5.00E-08 Analyst KYW2 :=ounting Uncertainty is calculated at the 68% confidence level (1-sigma). uCi/kg uCilkg Date 06/16/14 Result TC1 07/16/14 0634 1396265 TC1 07/15/14 1636 1396264 2 Time Prep Batch 1756 1396221 Analyst Comments Nominal Recove~% Acc~table Limits 115 (25%-125%) 96.7 (25%-125%) lij ij II Laboratories LLC a member of The GEL Group INC PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 May 22,2014 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: Vegetation Analysis Work Order: 347128 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on April21, 2014. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will fmd everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4505. Purchase Order: DW16138 Enclosures Sincerely, Heather Shaffer Project Manager llll'lllllllllllllllllllllllllllll www.gel.com Energy Fuels Resources (USA), Inc. Vegetation Analysis SDG: 347128 Case Narrative May 22,2014 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 347128 Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on April21, 2014 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following samples: Laboratory ID Client ID 347128001 North East 347128002 North West 347128003 South West Case Narrative: Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Heather Shaffer Project Manager Chain of Custody and Supporting Documentation Sheet 1 of 1 Samples Shipped to: Gel Laboratories Contact: Garrin Palmer ~2~0~40~S~av~a=g~e~R~o=a~d~--------------Ph:4356784115 Charleston, SC 29407 gpalmer@energyfuels.com Chain of Custody/Sampling Analysis Request Project s amplers N a me s amp ers s· •gna~t,~re Early Spring Vegetation I # ..__ ~ 2014 Garrin Palmer (:rvvv" Time Sample ID Date Collected Collected Laboratory Analysis Requested North East 4/16/2014 1245 Ra 226, PB 210 North West 4/16/2014 1315 Ra 226, PB 210 South West 4/16/2014 1400 Ra 226, PB 210 .. Please use caution when handling South West samples. Some cactus included in the samples. Comments: Relinquished By:(Signature) Garrin Palmer Date/TimeR 4/16/2014 1200 Relinquished By:(Signature) Date/Time - m:3!1[ Laboratories u~c SAMPLE RECEIPT & REVIEW FORM Client: 1~! \ I . SDG/ARICOC/Work Order: :Y-l 'l J L-)f Received By: t 1~"1QU I (!'{ Date Received: 042 1/ll I ~ ~ *If Net Counts> lOOcpm on samples not marked "radioactive", contact the Radiation Safety Group for further Suspected Hazard Information ;:.. ii_!.Yestigation. COC/Samples marked as radioactive? /' Maximum Net Counts Observed* (Obs.crvttl Counts~ Area U<~ckgrountl Count$); (_,{ {-1V\. Classified Radioactive II ol"ill by RSO? ../ 'fr )'CS, Were swipes taken of -sum1lle contatiners <action levels? I COC/Samples marked containing PCBs? ""' _/ Package, CDC. and/or Samples marked as / hc1~yllium 01 asbestos containing? / If yes, samples arc to be scgregeatecl as Safety Controlled Samples, and OIJened by the GEL Safety Group. Shipped as a DOT Hazardous'! / fj';zard Class Shl.pllCd: UN#: •. ~ruuruJ.W .. cdJts Forei1.m Sail? / Sample Receipt Criteria ~ ~ 0 Conm1ents/Qualifiers (Required for Non-Conforming Items) ;:.. z Shipping containers received intact I/ Circle Applicable: 1 Seals broken Damaged container Leaking container Other (describe) and sealed? / ~ Samples requiring cold preservation I~ I/ Preservation MeU10d: Ice bags Blue ice Dry ic~ (;~~Other (describe) 2 within (0 .::; 6 deg. C)?* / *all temperatures are recorded in 20 2a Daily check performed and passed on / Device Serial #: : k:irh~ ~ a.2f~L~rl/J IR temperature gun? I/ Secondary Tempemture Device · .1• ~1. 3 Chain of custody documents included ~ with shipment? Circle Applicable: 4 Sample containers intact and sealed? Seals broken Damaged container Leaking container Other (describe) Samples requiring chemical l.,/'1/ Sample !D's, containers affected and observed pH: 5 preservation at proper pH? If Preservation added. Lol#: VOA vials free of heads pace (defined ./ 1-Sample ID's and containers affected: 6 as < 6mm bubble)? 7 Are Encore containers present? I/ .~yes, immediately deliver to Volatiles laboratory) Samples received within holding I D's and tests nffcct~d: 8 time? ' 9 !Sample !D's on COC match llJ's on bottles? Date & time on COC match date & Sample ID's affected: 10 time on bottles? Number of containers received match Sample ID's affected: 11 number indicated on COC? 12 Are sample containers identifiable as / 1,.....- GEL provided? 13 COC form is properly signed in relinquished/received sections? Circle Applicable: FcdEx Air FedEx Ground UPS Field Services Courier Other !Z-/~{ ~l{y 02. Cf&Dlt 32.05 14 CatTier and tracking number. 97?9 ?Jqoq 901~ 57/'f Comments (Use Continuation Form if needed): ( . I t.-\ . « t.-. ~ t { ~f --r\---\ Dnlc~ 0-\_Lll'frage _j_, ·L l PM (or PMA) review: Initials ~ GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 347128 Early Spring Vegetation 2014 ClientSDG: Project Manager: Project Name: Purchase Order: Package Level: EDD Format: 347128 Heather Shaffer DNMI00101 Vegetation Analysis DW16138 LEVEL3 EIM_DNMI GELID Client Sample ID Client Sample Desc. 347128001 North East 347128002 North West 347128003 South West Collect Date & Time 16-APR-14 12:45 16-APR-14 13:15 16-APR-14 14:00 Work Order Due Date: 21-MAY-14 Package Due Date: EDD Due Date: Due Date: HXS1 Receive Time #of Date & Time Zone Cont. 21-APR-14 09:20 -2 21-APR-14 09:20 -2 21-APR-14 09:20 -2 1 18-MAY-14 20-MAY-14 21-MAY-14 Lab Matrix VEGETATION VEGETATION VEGETATION Report Date: 15-MAY-14 Work Order: 347128 Page 1 of 2 Collector: C Prelogin #: 20140415619 Project Workdef ID: 1310529 SDG Status: Closed Logged by: Fax Days to Due Date Process 30 30 30 CofC# Prelog Lab Field Group QC QC Client Sample ID Status Tests/Methods Product Reference Fax Date PM Comments Aux Data Receive Codes -001 North East -002 North West -003 South West REVW GFPC, Total Alpha Radium, solid REVW GFPC, Pb210, Solid REVW Laboratory Composite -Dry prep instructions REVW GFPC, Total Alpha Radium, solid REVW GFPC, Pb210, Solid REVW Laboratory Composite -Dry prep instructions REVW GFPC, Total Alpha Radium, solid REVW GFPC, Pb210, Solid REVW Laboratory Composite -Dry prep instructions Product: LABCOMP _S Workdef ID: 1310628 Method: In Product Group? No Product Description: Laboratory Composite -Dry prep instructions Samples: 001, 002, 003 Parmname Check: All parmnames scheduled properly CAS# Parmname use caution when handling; some cactus included in the sample. Group Name: Client Matrix Client Matrix Client Matrix Group Reference: SOLID SOLID SOLID Path: Rad Prep SPRP Product Reference: Moisture Correction: "As Received" Client RDL or PQL & Unit Reporting Units Parm Included Included Custom Function in Sample? in QC? List? No ~ \ GEL Laboratories LLC -Login Review Report Product: GFC_ PBS WorkdefiD: 1310600 In Product Group? No Method: DOE RP280 Modified Product Description: GFPC, Pb210, Solid Samples: 001, 002, 003 Parmname Check: All parmnames scheduled properly CAS# Parmname 14255-04-0 Lead-210 Product: GFCTORAS Workdef ID: 1310679 In Product Group? No Method: EPA 900.1 Modified Product Description: GFPC, Total Alpha Radium, solid Samples: 001, 002, 003 Parmname Check: All parmnames scheduled properly CAS# Parmname Total Radium Action Product Name Description Contingent Tests Login Requirements: Requirement Are these vegetation sample? Login Reminder? Group Name: Client RDL or PQL & Unit .000001 Group Name: Client RDL or PQL & Unit .00000005 Samples Reporting Units uCilkg Reporting Units uCi/kg Include? Comments Group Reference: Report Date: 15-MAY-14 Work Order:347128 Page 2 of 2 Path: Standard Product Reference: Moisture Correction: "As Received" Parm Included Included Custom Function in Sample? in QC? List? REG y y Group Reference: Path: Standard Product Reference: Yes Moisture Correction: "As Received" Parm Included Included Custom Function in Sample? in QC? List? REG y y Yes y y FOR VEGETATION: After logging in, change from DRY to WET in sample inquiry. FOR VEGETATION: After logging in, change from DRY to WET in sample inquiry. Log with lab comp. Peer Review by: ____________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? _____ _ Laboratory Certifications List of current GEL Certifications as of 22 May 2014 State Certification Alaska UST-110 Arkansas 88-0651 CLlA 4200904046 California NELAP 01151CA Colorado SC00012 Connecticut PH-0169 Delaware SC000122013-10 DoD ELAP/ ISO 17025 A2LA 2567.01 -Florida NELAP E87156 Foreign Soils Permit P330-12-00283,P330-12-00284 Georgia SC00012 -Georgia SDWA 967 --Hawaii scooo 122013-10 Idaho Chemistry SC00012 Idaho Radiochemistry SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 -Kentucky 90129 ·-Louisiana NELAP 03046 (AI33904) Louisiana SDWA LA130005 Maryland 270 Massachusetts M-SC012 Michigan 9976 Mississippi SC000122013-10 Nebraska NE -OS-26-13 -Nevada scooo 122014-1 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 -New York NELAP 11501 North Carolina 233 -North Carolina SDWA 45709 Oklahoma 9904 Pennsylvania NELAP 68-00485 Plant Material Permit PDEP-12-00260 South Carolina Chemistry 10120001 South Carolina GVL 23611001 South Carolina Radiochemi 10120002 Tennessee TN 02934 TexasNELAP Tl04704235-14-9 Utah NELAP scooo 1220 13-11 Vermont VT87156 Virginia NELAP 460202 Washington C780-12 Wisconsin 999887790 Method/ Analysis Information Radiochemistry Case Narrative Energy Fuels Resources (DNMI) SDG 347128 Product: GFPC, Total Alpha Radium, solid Analytical Method: EPA 900.1 Modified Prep Method: Dry Soil Prep Analytical Batch Number: Prep Batch Number: 1385421 1382146 SampleiD 347128001 347128002 347128003 1203081581 1203081582 1203081583 1203081584 Client ID North East North West South West Method Blank (MB) 347128002(North West) Sample Duplicate (DUP) 347128002(North West) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-010 REV# 15. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control (OC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 347128002 (North West). QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The blank, 1203081581 (MB), did not meet the detection limit due to keeping the blank volume consistent with the other sample aliquots. All other samples met the detection limits. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set. Recounts None of the samples in this batch were recounted. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Sample-Specific MDAIMDC The MD A/MDC reported on the certificate of analysis is a sample-specific MD A/MDC. Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required. Method/ Analysis Information Product: GFPC, Pb210, Solid Analytical Method: DOE RP280 Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1385433 Prep Batch Number: 1382146 Sample ID Client ID 347128001 347128002 347128003 1203081601 1203081602 1203081603 1203081604 North East North West South West Method Blank (MB) 347128002(North West) Sample Duplicate (DUP) 347128002(North West) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-018 REV# 13. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 347128002 (North West). QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The blank, 1203081601 (MB), did not meet the detection limit due to keeping the blank volume consistent with the other sample aliquots. All other samples met the detection limits. The sample and the duplicate, 1203081602 (North West) and 347128002 (North West), did not meet the relative percent difference requirement; however, they do meet the relative error ratio requirement with value of 1. 71. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep!Re-analysis None of the samples in this sample set required reprep or reanalysis. Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set. Recounts Samples 1203081603 (North West) and 1203081604 (LCS) were recounted due to high recovery. The recounts are reported. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Sample-Specific MDA/MDC The MD A/MDC reported on the certificate of analysis is a sample-specific MD A/MDC. Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMIOOl Energy Fuels Resources (USA), Inc. Client SDG: 347128 GEL Work Order: 347128 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. Review/Validation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: ~~-;1 ~ Date: 28 MAY 2014 Name: Theresa Austin Title: Group Leader GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407-(843) 556-8171 -www.gel.com QC Summary Contact: Workorder: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Ms. Kathy Weinel 347128 Parmname Rad Gas Flow NOM Sample Qual QC 3atch 1385421 QC1203081582 347128002 DUP Total Radium 2.53£-05 Uncertainty +/-6.29£-07 QC1203081584 LCS Total Radium 0.000886 Uncertainty QC1203081581 MB Total Radium u Uncertainty QC1203081583 347128002 MS Total Radium O.OOII 2.53£-05 Uncertainty +/-6.29£-07 3atch 1385433 QC 1203081602 347128002 DUP Lead-210 5.70£-05 Uncertainty +/-2.21£-06 QC1203081604 LCS Lead-210 0.00173 Uncertainty QC1203081601 MB Lead-210 u Uncertainty QC1203081603 347128002 MS Lead-210 0.00212 5.70£-05 Uncertainty +/-2.21£-06 Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product 2.83£-05 +/-6.38£-07 0.000797 +/-9.28£-06 -1.36£-07 +/-2.99£-07 0.00092 +/-I.OOE-05 8.08£-05 +/-2.55£-06 0.00202 +/-2.61£-05 2.78£-06 +/-2.98£-06 0.00258 +/-3.27£-05 Units uCi/kg uCi/kg uCi/kg uCi/kg uCi/kg uCi/kg uCi/kg uCi/kg RPD% 11.3 34.5* A B BD c D F H For General Chemistry and Organic analysis 'the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Reoort Date: May 28, 2014 Page 1 of REC% Range Anlst Date Time (0%-20%) KSDI 05/27/14 15:5 89.9 (75%-125%) 05/27/14 16:2 05/27/14 15:5 81.3 (75%-125%) 05/27/14 15:5 (0%-20%) KSDI 05/27/14 16:5 ]]6 (75%-125%) 05/28/14 ll:O 05/27/14 16:5 ]]9 (75%-125%) 05/28/14 II :0 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407-(843) 556-8171 -www.gel.com QC Summary Workorder: 347128 Parmname NOM Sample ual ~c Units RPD% K Analyte present. Reported value may be biased high. Actual value is expected to be lower. L Analyte present. Reported value may be biased low. Actual value is expected to be higher. M M if above MDC and less than LLD M Matrix Related Failure N/A RPD or %Recovery limits do not apply. See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative orDER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification REC% Range Anlst Nl NO NJ Q R u Ul UJ UL X y Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier 1\ h QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of Date Time N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. 1\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +I-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SOIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. [ij#ul Laboratories LLc a member of The GEL Group INC PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 July 18,2014 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: Vegetation Analysis Work Order: 350589 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on June 13,2014. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4505. Purchase Order: DW16138 Enclosures Sincerely. Heather Shaffer Project Manager www.gel.com Energy Fuels Resources (USA), Inc. Vegetation Analysis SDG: 350589 Case Narrative July 18, 2014 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 350589 Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on June 13,2014 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following samples: Laboratory ID Client ID 350589001 North East 350589002 North West 350589003 South West Case Narrative: Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Heather Shaffer Project Manager Chain of Custody and Supporting Documentation 3~589 Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: Gel Laboratories Contact: Garrin Palmer ~2~0~40~S-av_a_g_e~R~o-a-d~--------------Ph:4356784115 Charleston, SC 29407 gpalmer@energyfuels.com Chain of Custody/Sampling Analysis Request p . roJect S -I N amp1ers arne s amp ers s· t 1gna ure Late Spring Vegetation I G-c~P~ 2014 Garrin Palmer Time Sample ID Date Collected Collected Laboratory Analysis Requested North East 6/10/2014 5571 Ra 226, PB 210 North West 6/10/2014 5220 Ra 226l PB 210 South West 6/10/2014 4950 Ra 226, PB 210 * Please use caution when handling South West samples. Some cactus included in the samples. Comments: Rennquished By:(Signature) Datemme Received By:{Signature) Date/Tfme Garrin PalmL 6/10/2014 C1rr (6 .. J3 ·J•-"( &~"R 1000 0'/10 Relinquished By:(Signature) Date/Time Recei~ed By:(Signature) Datemme < m3) /Laboratories Lt.c SAMPLE RECEIPT & REVIEW FORM Client: Df'\ffi\ SDG/ARJCOC/Work Order: 3Sos~ Received By: uP Date Received: u-1.3· Jl.{ Suspected Hazard Information ., Q "'IfNet Counts> IOOcpm on samples not marked "radioactive", contact the Radiation Safety Group for further ~ z investigation . COC/Samples marked as radioactive? ./ Maximum Net Counts Observed• (Observed Counts-Area Background Counts): OcaY\ Classified Radioactive II or Ill by RSO? v If yes, Were swipes taken of sample contatiners <action levels? I COC/Samples marked containing PCBs? / Package, COC, and/or Samples marked as I/ beryllium or asbestos containing? If yes, samples are to be scgrogcllled.as Sarcty Controlled Snmplcs, and opened by the GEL Safety Group. Shipped as a DOT Hazardous? i/ ~azard Class Shipped: UN#: Samples identified as Foreign Soil? i/ Sample Receipt Criteria :E ~ ~ Comments/Qualifiers (Required for Non-Conforming Items) Shipping containers received intact ,V Circle Applicable: 1 Seals broken Damaged container Leaking container Other (describe) and sealed? ...-""'h Samples requiring cold preservation I--Preservation Method: Ice bags Blue ice Dry ice Ce~~ther (describe) 2 within (0 < 6 deg. C)?"' / (~ •all temperatures are recorded in 2a I Daily check performed and passed on (I-11 DeviceSerialll: ~~al !~~Lt l IIR temperature gun? Secondary Temperature Device 3 Chain of custody documents included J with shipment? Circle Applicable: 4 Sample containers intact and sealed? Seals broken Damaged container Leaking container Other (describe) • 5 Samples requiring chemical / S3mplc !D's, containers affected and observed pH: preservation at proper pH? lfrtn.ntld~•l LtiW' VOA vials free ofheadspace (defined /~ Sample !D's nnd containers affected: 6 as< 6mm bubble)? pfyes, ;mmP<HotPiv deliver to Volatiles oaooraroryJ 7 Are Encore containers present? I/ Samples received within holding ID'sandtes~affected: 8 time? .I Sample ID's on COC match ID's on I Sample: !D's and containers affected: 9 oomes? Date & time on CDC match date & Sample I'D's uffectcd: 10 time on bottles? / ··tl'ff\1 OY\ C-lW'\tcU ~~ sw 014$ t\lW t'l~ IS .vE'~ ~ Number of containers received match I Sample !D's affected: 11 number indicated on COC? ID 1"'\V'\.P V).ef Are sample containers identifiable as ' 12 I GEL provided? 13 COC form is properly signed in /I relinquished/received sections? --~FolE<Gro'"d Cir~Iicable: PS Field Services Courier Other g(-> qot~ qq3( Iz_ 187 l/~Y 12 14 Carrier and tracking number. qoyq 27~2 I ( I l 9Lf '2lo 21S3 (Use Continuation Form if needed): PM (or PMA) review: Initials '--»P Date l.o-J1~JU Page_j r__j_ v GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 350589 Client SDG: 350589 Project Manager: Project Name: Purchase Order: Package Level: EDD Format: Heather Shaffer DNMI00101 Vegetation Analysis DW16138 LEVEL3 EIM_DNMI GELID Client Sample ID Client Sample Desc. 350589001 North East 350589002 North West 350589003 South West Collect Date & Time 10-JUN-14 08:45 10-JUN-14 08:15 10-JUN-14 07:45 Work Order Due Date: 21-JUL-14 Package Due Date: EDD Due Date: Due Date: HXT1 Receive Time #of Date & Time Zone Cont. 13-JUN-14 09:20 -2 13-JUN-14 09:20 -2 13-JUN-14 09:20 -2 18-JUL-14 20-JUL-14 21-JUL-14 Lab Matrix VEGETATION VEGETATION VEGETATION Report Date: 18-JUL -14 Work Order: 350589 Page 1 of 2 Collector: C Prelogin #: 20140617731 Project Workdef ID: 1310529 SDG Status: Closed Logged by: Fax Days to Due Date Process 30 30 30 CofC# Prelog Lab Field Group QC QC Client Sample ID Status Tests/Methods Product Reference Fax Date PM Comments Aux Data Receive Codes -001 North East -002 North West -003 South West REVW GFPC, Total Alpha Radium, solid REVW GFPC, Pb210, Solid REVW Laboratory Composite -Dry prep instructions REVW GFPC, Total Alpha Radium, solid REVW GFPC, Pb210, Solid REVW Laboratory Composite -Dry prep instructions REVW GFPC, Total Alpha Radium, solid REVW GFPC, Pb210, Solid REVW Laboratory Composite -Dry prep instructions Product: LABCOMP _S Workdef ID: 1310628 Method: In Product Group? No Product Description: Laboratory Composite -Dry prep instructions Samples: 001, 002, 003 Parmname Check: All parmnames scheduled properly CAS# Parmname Group Name: Client RDL or PQL& Unit Cooler Seal Undisturbed Temperature (C) Cooler Seal Undisturbed Temperature (C) Cooler Seal Undisturbed Temperature (C) Group Reference: y 19 y 19 y 19 Path: Rad Prep SPRP Product Reference: Moisture Correction: "As Received" Reporting Units Parm Included Included Custom Function in Sample? in QC? List? 'No GEL Laboratories LLC -Login Review Report Product: GFC_ PBS Workdef ID: 1310600 In Product Group? No Method: DOE RP280 Mod ified Product Description: GFPC, Pb210, Solid Samples: 001, 002, 003 Parmname Check: All parmnames scheduled properly CAS# Parmname 14255-04-0 Lead-210 Product: GFCTORAS WorkdefiD: 1310679 In Product Group? No Method: EPA 900.1 Modified Product Description:: GFPC, Total Alpha Radium, solid Samples: 001, 002, 003 Parmname Check: All parmnames scheduled properly CAS# Parmname Total Radium Action Product Name Description Contingent Tests Login Requirements: Requirement Are these vegetation sample? Login Reminder? Group Name: Client RDL or PQL & Unit .000001 Group Name: Client RDL or PQL & Unit .00000005 Samples Group Reference: Report Date: 18-JUL-14 Work Order: 350589 Page 2 of 2 Path: Standard Product Reference: Moisture Correction: "As Received" Reporting Parm Included Included Custom Units Function in Sample? in QC? List? uCilkg REG y y Yes Group Reference: Path: Standard Product Reference: Moisture Correction: "As Received" Reporting Parm Included Included Custom Units Function in Sample? in QC? List? uCi/kg REG y y Yes Include? Comments y y FOR VEGETATION: After logging in, change from DRY to WET in sample inquiry. FOR VEGETATION: After logging in, change from DRY to WET in sample inquiry. Log with lab comp. Peer Review by: ___________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? _____ _ Laboratory Certifications List of current GEL Certifications as of 18 July 2014 State I Certification l Alaska I UST-110 I Arkansas 88-0651 ·-' CLIA 42D0904046 California NELAP 01151CA Colorado SC00012 -Connecticut PH-0169 Delaware scooo 122013-10 DoD ELAP/ ISO 17025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-12-00283,P330-12-00284 Georgia SC00012 Georgia SDWA 967 Hawaii scooo 122013-10 Idaho Chemistry SC00012 Idaho Radiochemistry SC00012 lllinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky 90129 Louisiana NELAP 03046 (AI33904) Louisiana SDWA LA130005 Maryland 270 Massachusetts M-SCOI2 Michigan 9976 Mississippi SC000122013-10 Nebraska NE-OS-26-13 Nevada scooo 122014-1 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SCOOOI2 New YorkNELAP 11501 North Carolina 233 North Carolina SDWA 45709 r-Oklahoma 9904 Pennsylvania NELAP 68-00485 Plant Material Permit PDEP-12-00260 South Carolina Chemistry 10120001 South Carolina GVL 23611001 South Carolina Radiochemi 10120002 Tennessee TN 02934 TexasNELAP T104704235-14-9 UtahNELAP scooo 122014-13 Vermont VT87156 Virginia NELAP 460202 Washington C780-12 Wisconsin 999887790 . "' Method/ Analysis Information Radiochemistry Case Narrative Energy Fuels Resources (DNMI) SDG 350589 Product: GFPC, Total Alpha Radium, solid Analytical Method: EPA 900.1 Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1396264 Prep Batch Number: 1396221 Sample ID 350589001 350589002 350589003 1203110048 1203110049 1203110050 1203110051 Client ID North East North West South West Method Blank (MB) 350589001(North East) Sample Duplicate (DUP) 350589001(North East) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-010 REV# 15. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control <QC) Information: Blank Information The blank volume is representative of the sample volume in this batch . Designated QC The following sample was used for QC: 350589001 (North East). QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The blank, 1203110048 (MB), did not meet the detection limit due to keeping the blank volume consistent with the other sample aliquots. All other samples met the detection limits. The blank, 1203110048 (MB), result is greater than the required detection limit but less than the MDC. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Chern ical Recoveries All chemical recoveries meet the required acceptance limits for this sample set. Recounts None of the samples in this sample set were recounted. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Sample-Specific MDA!MDC The MD A/MDC reported on the certificate of analysis is a sample-specific MD A/MDC. Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required. Method/Analysis Information Product: GFPC, Pb210, Solid Analytical Method: DOE RP280 Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1396265 Prep Batch Number: 1396221 Sample ID 350589001 350589002 350589003 1203110052 1203110053 1203110054 1203110055 Client ID North East North West South West Method Blank (MB) 35058900l(North East) Sample Duplicate (DUP) 350589001(North East) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-018 REV# 13. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Ouality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 350589001 (North East). QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The blank, 1203110052 (MB), did not meet the detection limit due to keeping the blank volume consistent with the other sample aliquots. All other samples met the detection limits. The blank 1203110052 (MB) result is greater than the required detection limit but less than the MDC. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep!Re-analysis None of the samples in this sample set required reprep or reanalysis. Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set. Recounts None of the samples in this sample set were recounted. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Sample-Specific MDA/MDC The MD A/MDC reported on the certificate of analysis is a sample-specific MD A/MDC. Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. ,.. .... GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMIOOl Energy Fuels Resources (USA), Inc. Client SDG: 350589 GEL Work Order: 350589 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. ReviewN alidation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: ~~ Name: Kate Gellatly Date: 18 JUL 2014 Title: Analyst I GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407-(843) 556-8171 -www.gel.com Contact: Workorder: Parmname Rad Gas Flow Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Ms. Kathy Weinel 350589 NOM 3atch 1396264 QC1203110049 350589001 DUP Total Radium 2.60E-05 Uncertainty +/-8.46E-07 QC1203110051 LCS Total Radium 0.00104 Uncertainty QCI203110048 MB Total Radium Uncertainty QC1203110050 350589001 MS Total Radium 0.0023 2.60E-05 Uncertainty +/-8.46£-07 3atch 1396265 QC1203110053 350589001 DUP Lead-210 5.60E-05 Uncertainty +/-3.08£-06 QC1203110055 LCS Lead-210 0.00202 Uncertainty QCI203110052 MB Lead-210 Uncertainty QC1203110054 350589001 MS Lead-210 0.00442 5.60E-05 Uncertainty +/-3.08£-06 Notes: QC Summary QC Units 2.35E-05 uCi/kg +/-8.07£-07 0.000855 uCi/kg +/-1.06E-05 u 3.62E-07 uCi/kg +/-1 .53E-07 0.00182 uCi/kg +/-1.96£-05 4.87E-05 uCilkg +/-2.75£-06 0.00222 uCi/kg +/-3 .08£-05 u 2.41E-06 uCi/kg +/-1 .56£-06 0.00486 uCi/kg +/-6.11 E-05 Counting Uncertainty is calculated at the 68% confidence level (!-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product RPD% 10.0 13.9 A B BD c D F H For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GCIMS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Reoort Date: July 18, 2014 Page 1 of REC% Ran e An-=ls..:...t __ D=at:..:.e__;:T...;cim==-e (0%-20%) TCI 07/15/14 16:3 82.4 (75%-125%) 07/15/14 16:3• 07/15/14 16:3· 77.9 (75%-125%) 07/15/14 16:3· (0%-20%) TCl 07/16114 06:J 110 (75%-125%) 07/16/14 06:3' 07/16/14 06:3· 109 (75%-125%) 07116/14 06:J GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407-(843) 556-8171 -www.gel.com QC Summary Workorder: 350589 Parmname NOM Sample Qual QC Units RPD% K Analyte present. Reported value may be biased high. Actual value is expected to be lower. L Analyte present. Reported value may be biased low. Actual value is expected to be higher. M M if above MDC and less than LLD M Matrix Related Failure N/A RPD or %Recovery limits do not apply. See case narrative Analyte concentration is not detected above the detection limit Nl ND NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative orDER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification REC% Q R u UI UJ UL X y Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound Anlst 1\ h RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of Date Time N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. 1\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. ATTACHMENT G STACK SAMPLE LABORATORY RESULTS Prepared for: Energy Fuels Resources 6425 S Hwy 91 Blanding, Utah 84511 Date of Report: January 30, 2014 FIRST QUARTER RADIONUCLIDE EMISSIONS TEST CONDUCTED AT ENERGY FUELS RESOURCES SOUTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE BLANDING, UTAH January 14-15, 2014 by: TETCO 391 East 620 South American Fork, UT 84003 Phone (801) 492-9106 Fax (801) 492-9107 fax .· '· l ., 1 -' ' . il: .. ~ ·~ 1. • CERTIFICATION OF REPORT INTEGRITY Technical Emissions Testing Company (TETCO) certifies that this report represents the truth as well as can be derived by the methods employed. Every effort was made to obtain accurate and representative data and to comply with procedures set forth in the Federal Register. Dean Kitchen Reviewer: /b~ c?' ~ ---------;rp~==~~~?~~=----- Date: ______ !_-~):_,_9_----4--,J-ri-- Reviewer: _ _,_~....:..._....--_.fh_· _________ 0 _ 0 u_g_ 0 _ 1 s-en Date:_......:....\ \.:....:....;--+v\-.!1~----- ii .. TABLE OF CONTENTS PAGE Introduction Test Purpose ......................................................................................................................... 1 Test Location and Type of Process ...................................................................................... 1 Test Dates ............................................................................................................................. I Pollutants Tested and Methods Applied .............................................................................. } Test Participants ................................................................................................................... 2 Deviations from EPA Methods ............................................................................................ 2 Quality Assurance ................................................................................................................ 2 Summary of Results Emission Results .................................................................................................................. 3 Process Data ......................................................................................................................... 3 Description of Collected Samples ....................................................................................... .3 Discussion of Errors or Irregularities ................................................... , ....... , ....................... 3 Percent Isokinetics ............................................................................................................... 4 Source Operation Process Control Devices Operation ..................................................................................... 5 Process Representativeness ............................................................................................ ' ........ 5 Sampling and Analysis Procedures Sampling Port Location ....................................................................................................... 6 Sampling Point Location ...................................................................................................... 6 Sampling Train Description ................................................................................................. 6 Sampling and Analytical Procedures ................................................................................... 7 Quality Assurance ................................................................................................................ ? Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence iii LIST OF TABLES Table I Measured Radionuclide Emissions ..................................................................................... .3 II Percent Isokinetics ................................................................................................................ 4 III Sampling Point Location ...................................................................................................... 6 IV Complete Results, South Yell ow Cake Scrubber .............................................. Appendix A V Complete Results, Yell ow Cake Dryer Baghouse ............................................. Appendix A LIST OF FIGURES Figure 1 Facility Schematic Representation South Yellow Cake Scrubber ..................... Appendix D 2 Facility Schematic Representation Yellow Cake Dryer Baghouse .................... Appendix D 3 Schematic of Method 5/114 Sampling Train ..................................................... Appendix E iv INTRODUCTION Test Purpose This test project was conducted to determine the total radionuclide emissions from the South Yell ow Cake Scrubber and the Yell ow Cake Dryer Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dscf). These tests were for U-Nat only. Test Location and Type of Process Energy Fuels Resources is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Yellow Cake Dryer Baghouse. The packaging enclosure also discharges into the Yellow Cake Dryer Baghouse. The South Yellow Cake (SYC) dryer was the only operating dryer at the time ofthe test. The North Yellow Cake dryer is currently not operational. The Grizzly Baghouse serves as the main dust control device for the raw ore unloading and conveying to the processing building. Stack schematics are shown as Figures 1 and 2 in Appendix D. Test Dates The first test run on the SYC Scrubber was completed January 14, 2014 and the second run on January 15,2014. One run was completed on the Yellow Cake Dryer Baghouse January 15, 2014. Pollutants Tested and Methods Applied The tests were a determination ofradionuclide emissions in accordance with EPA Method 5/114. Test run filters and front wash residues were sent to Test America located in Richland, Washington for radionuclide analysis. Test Participants Test Facility State Agency TETCO : Garrin Palmer None Doug Olsen Jeff Graton Deviations From EPA Methods None. Quality Assurance Mike McNamara Testing procedures and sample recovery techniques were according to those outlined in the Federal Register and the Quality Assurance Handbook for Air Pollution Measurement Systems. 2 SUMMARY OF RESULTS Emission Results Table I presents the findings of the test in Curies per dry standard cubic foot. Tables IV-VI in Appendix A have more detailed information. Table I. Measured Radionuclide Emissions Run# 1 2 AVE Process Data South Yell ow Cake Scrubber pCi/dscf 7.17 7.80 7.49 pCilhr 5.921E +05 6.748E+05 6.334E+OS Yell ow Cake Dryer Baghouse pCi/dscf pCilhr 27.92 6.596E+06 27.92 6.596E+06 The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow, pressure drop readings (..::lp) were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (..::lp) were recorded and are found on the test run sheets. Production data will be submitted by Energy Fuels Resources. Description of Collected Samples The test filters for the South Yell ow Cake Scrubber were heavily covered with a white colored particulate. The front washes were cloudy in appearance. The test filters for the Yell ow Cake Dryer Baghouse were lightly colored with a tan colored particulate. The front wash was clear in appearance. Discussion of Errors or Irregularities None 3 Percent Isokinetic Sampling Each test run was isokinetic within the ±10% of 100% criterion specified in the Federal Register. Isokinetic values for each test run are presented in Table II. Table II. Percent Isokinetic Sam Run# 2 South Yell ow Cake Scrubber 99 99 4 Yell ow Cake Dryer Baghouse 97 .-., • • • T L ·, . ·.·- • ' • 4 ~ ~--·--.. --···-_....__ SOURCE OPERATION Process Control Devices Operation All process control devices were operated normally. Recorded scrubber water flow, pressure and baghouse ~p readings were recorded and are found on the test run sheets or in Appendix D. Process Representativeness The facility was operated normally. Production data was retained by Energy Fuels Resources. 5 SAMPLING AND ANALYSIS PROCEDURES Sampling Port Location The inside diameter ofthe South Yellow Cake Scrubber stack is 12.75 inches. The two, four-inch diameter sample port are located 28.24 diameters (30 feet) downstream from the last disturbance and 6.59 diameters (7 feet) upstream from the next disturbance. Figure 1 in Appendix Dis a schematic of the stack. The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch diameter sample ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 2 in Appendix D. Sampling Point Location Table III shows the distance of each sampling point from the inside wall according to EPA Method 1. Each point is marked and identified with a wrapping of glass tape and numbered. These points are determined by measuring the distance from the inside wall. Distance (inches) from Inside Wall Sample Point SYC Scrubber Dryer Baghouse 1 2 3 4 5 6 Sampling Train Description 0.85 3.19 9.56 11.90 [-. . t . ~~,~-·, --r•· ,-~·~~ 1' •• ·j/ ::..:. ... _----.__ --·.:. 0.70 2.34 4.74 11.26 13.66 15.30 To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-51114 were followed. All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent interference ofthe sampled gas and particulate. The stack analyzers used to conduct Methods 1- 6 5/114 are constructed to meet the specifications outlined in the CFR. The temperature sensors are K-type thermocouples. Heater, vacuum and pitot line cmmections have been designed to be interchangeable with all units used by the tester. A 316 stainless steel probe liner was used for the tests. Figure 4 in Appendix Eisa sketch of the Methods 5/114 sampling train. Sample boxes were prepared for testing by following the prescribed procedures outlined in Methods 5/114. Sampling and Analytical Procedures All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 5/114. Quality Assurance All equipment setup, sampling procedures, sample recovery and equipment calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbook for Air Pollution Measurement Systems. 7 APPENDIX A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence 8 APPENDIX A Table IV Complete Results, South Yellow Cake Scrubber Table V Complete Results, Yellow Cake Dryer Baghouse Nomenclature Sample Equations A • SVC Scrubbor .. ~ TABLE IV .. • .J. COMPLETE RESULTS ENERGY FUELS CORPORATION, BLANDING, UTAH SOUTH YELLOWCAKE SCRUBBER EXHAUST Symbol Descrietion Dimensions Run #J Run #2 Date 1/14/2014 1/15/2015 Filter# 6108 6112 Begin Time Test Began 9:55 7:49 End Time Test Ended 18:17 16:11 Pbm Meter Barometric Pressure ln. Hg. Abs 24.75 24.75 .1-H Orifice Pressure Drop ln. H20 1.518 1.707 y Meter Calibration Y Factor dimensionless 1.002 1.002 Vm Volume Gas Sampled-Meter Conditions cf 377.457 395.092 Tm Avg Meter Temperarure "F 84.9 85.4 V.1.P Sq Root Velocity Head Root in H20 0.5517 0.5842 Wt.vc Weight Water Collected Grams 421.6 498.8 T, Duration ofT est Minutes 480 480 cp Pita! Tube Coefficient Dimensionless 0.84 0.84 Dn Nozzle Diameter Inches 0.2755 0.2755 C02 Volume %Carbon Dioxide Percent 1.10 2.00 02 Volume% Oxygen Percent 18.90 18.00 N2 &CO Volume% Nitrogen and Carbon Monoxide Percent 80.00 80.00 Ymsrd Volume Gas Sampled (Standard) dscf 304.524 318.637 Vw Volume Water Vapor scf 19.878 23.518 B W s (measured) Frnction H20 in Stack Gas (Measured) Fraction 0.061 0.069 Bws (saturated) Fraction H20 in Stack Gas (Saturated) Fraction 0.084 0.090 Bw. Fraction H10 in Stack Gas * Fraction 0.061 0.069 xd Fraction of Dry Gas Fraction 0.939 0.931 Md Molecular Wt. Dry Gas lbllbmol 28.93 29.04 M. Molecular Wt. Stack Gas lbllbmol 28.26 28.28 %1 Percentlsokinetic Percent 98.8 98.6 AVG T. Avg Stack Temperature OF 102.5 104.5 103.5 As Stack Cross Sectional Area Sq. Ft. 0.887 0.887 Po Stack Static Pressure ln. H20 -0.310 -0.310 PbP Sample Pon Barometric Pressure ln. Hg Abs 24.68 24.68 P. Stack Pressure ln. Hg. Abs 24.657 24.657 Q. Stack Gas Volumetric Flow Rate (Sid) dscfin 1.38E+03 1.44E+03 1.4IE+03 Q. Stack Gas Volumetric Flow Rate (Actual) cfin 1.89E+03 2.01E+03 1.95E+03 v. Velocity of Stack Gas fpm 2.14E+03 2.26E+03 2.20E+03 Curies Radionuclides per sample pCi 2184.5 2485.2 Crad Concentration of Radio nuclides pCi/dscf 7.173 7.799 7.486 ERrad Emission Rate ofRadionuclides pCi/hr 5.921E+05 6.748E+05 6.334E+05 * If the measured moisture content is greater than the saturated moisture level (supersaturated), the saturated moisture value will be used in all calculations (40 CFR 60, Method 4, Section 12. I. 7). Symbol Date Filter# Begin End Pbm ilH y Vm Tm .YilP Wfwc T, cp Dn C02 02 N2 &CO Ymstd Vw Bw5 xd Md M, %1 T. A, Pa PbP Ps Q, Q. v. Curies Crad ERrad f . ";. f Ti\BLEV COMPLETE RESULTS, PM ENERGY FUELS CORPORATION, BLANDING, UTAH YELLOW CAKE DRYER BAGHOUSE Descri~tion Dimensions Run #I Dale 1115/2014 6107 Ttme Test Began 10:57 Time Test Ended 13:0 I Meter Barometric Pressure ln. Hg. Abs 24.75 Orifice Pressure Drop ln. H20 2.033 Meter Calibration Y Factor dimensionless 1.002 Volume Gas Sampled-· Meter Conditions cf 108.674 Avg Meter Temperalure "F 77.6 Sq Root Velocily Head Root In_ H,O 0.9327 Weight Water Collected Grams 6.9 Duration of Test Minutes 120 Pilot Tube Coefficient Dimensionless 0.84 Nozzle Diameter Inches 0.2230 Volume% Carbon Dioxide Percent 0.00 Volume% Oxygen Percent 20.90 Volume% Nitrogen and Carbon Monoxide Percent 79.10 Volume Gas Sampled (Standard) dscf 89.002 Volume Water Vapor scf 0.325 Fraction HP in Stack Gas Fraction 0.004 Fraction of Dry Gas Fraction 0.996 Molecular Wt. Dry Gas lbllbmol 28.84 Molecular Wt. Stack Gas lb/lbmol 28.80 Percenllsokinelic Percent 97.0 Avg Stack Temperature "F 75.9 Stack Cross Sectional Area Sq. Ft. 1.396 Stack Static Pressure ln. H20 -1.30 Sample Port Barometric Pressure ln. Hg Abs 24.68 Stack Pressure ln. Hg. Abs 24.584 Stack Gas Volumetric Flow Rate (Sid) dscfm 3.94E+03 Stack Gas Volumetric Flow Rate (Actual) cfm 4.88E+03 Velocily of Stack Gas fpm 3.50E+03 Radionucl ides per sample pCi 2485.2 Concentration of Radionuclides pCildscf 27.923 I Emission Rate of Radionuclides pCilhr 6.596E+06 Dryer Bag house 13 General Npmenclature %1 = percent isokinetic, percent A.=(D/14)•1t AStlP = see VilP Btu = unit heat value (British thennal unit) Bws = fraction of water in stack gas (may have designation of "measured" or "saturated") "measured" represents measured moisture based upon sample volume and water collected "saturated" is a calculated value based upon stack pressure and temperature C0 = average of initial and final system zero gas calibration bias checks (ppm, percent) Cavg = average gas concentration (as measured) C8 = concentration of particulate matter, back half(gr/dscf,lb/dscf, etc.) Ccand = concentration of condensibles (grain/dscf) Ccors = concentration of coarse particulate (gr/dscf) Coor = measured concentration of a calibration gas when introduced in direct calibration mode Cr. = concentration of particulate matter, front half, actual stack flow (gr /act) CF = concentration of particulate matter, front half (gr/dscf,lb/dscf, etc.) C805 = Cavs corrected for initial and final system bias checks (Equation 7E-5) Cm = average of initial and final system upscale gas calibration bias checks (ppm, percent) Cma = actual concentration of upscale calibration gas Cmetal = concentration of metals (ppm, 11glfe, etc.) atomic symbol replaces "metal" C02 = percent carbon dioxide in the stack gas CP = pitot tube coefficient (0.84) Cp~110 = concentration ofPM10 particulate (gr/dscf) C,.d = concentration ofradionuclides (pCi/dscf) CS = measured concentration of a calibration gas when introduced in system calibration mode Cx = Any species symbol may replace X. Units may be expressed as ppm, lb/dscf, etc. Cx (corr) = actual gas concentration corrected to required percent 0 2 Curies= Measured radionuclides per sample. Units may be pCi or uCi. De= jet diameter (em) DIF = Dioxins and Furans (See laboratory report for DIF descriptions and nomenclacture) tlH = orifice pressure drop (inches H20) tlH@ = orifice pressure (inches H20) t1Hd = orifice pressure head (inches H20) needed for impactor flow rate Dn = nozzle diameter (inches) tlP = stack flow pressure differential (inches H20) Dp50 = 50% effective cutoff diameter of particle (em) D.= diameter of the stack (feet) EA = percent excess air ER8 = emission rate of back half particulate (lblhr) ERcond = emission rate of condensibles (lblhr) ERcors = emission rate of coarse particulate (lblhr) ERF = emission rate affront half particulate (lb/hr) ER~a.r = emission rate of a gas (lblhr) ERmmBtu = emission rate per mmBtu of fuel ERpt.11o = emission rate ofPM10 particulate (lblhr) ERrad = emission rate of radionuclides (pCilhr) ER~ = emission rate of compound which replaces X. Units are usually in lblhr. F0 = Dry based fuel factor. Ratio of the gas volume of the products of combustion to the heat content See 40 CFR 60, Appendix A, Method 19, Table 19-2 for fuel factor values. Kc = Cunningham slip correction factor A.= mean free path of molecules in gas phase (em) mmBtu = million Btu .. General Nomenclature Mcond = mass ofcondensibles (milligrams) Mco" = mass of coarse particulate (milligrams) Md = molecular weight of stack gas, dry basis (lb/lb-mol) Mr = mass of particulate on filter (mg) Mrp = mass of particulate matter on filter and probe (mg) mmBtu = million Btu Mp = mass of particulate matter in probe and front wash (mg) MPMIO = mass ofPM10 particulate (milligrams) M, = molecular weight of stack gas, wet basis (lb/lbmol) Mx = mass of species "X". Units may vary and other descriptive subscripts may apply. J..ls = gas viscosity (poise) Mwx = molecular weight of gas species (g/gmol) N = number of jets per plate N2 = percent nitrogen in the stack gas 0 2 = percent oxygen in the stack gas ..J/lP = average of the square roots of /lP (may also be referred to as AS/lP} ..Jflp1 = square root of llP at point I of the current test, Method 20 I A ..J/lP 1' = square root of /lP at point I of the previous traverse, Method 20 I A ..J/lP'ave = average of the square roots of /lP from the previous traverse, Method 20 I A Pbm = absolute barometric pressure at the dry gas meter (inches Hg) Pbp = absolute barometric pressure at the sample location (inches Hg) P0 = stack static pressure (inches H20) P5 = absolute stack pressure (inches Hg) P51d = absolute pressure at standard conditions (29.92 inches Hg.) e = time of test (minutes) 81 = sample time (duration in minutes) at first sample point for Method 20IA 8n = sample time (duration in minutes) at sample point "n" for Method 20IA 81esr= target test time for Method 201A (minutes) Oa = stack gas volumetric flow rate (acfm) Q, = stack gas volumetric flow rate (dscfm) Osc = actual gas flow rate through the cyclone (acfm) Osee = actual gas flow rate through the impactor (acfm) Ow= wet stack gas std . volumetric flow ere/min, wscfm) R = gas constant (2 I .85 inches Hg*ft3/(lbmol*R)) Pp = particle density (I g/cm3) Ps = stack gas density (g/cm3) T m = stack temperature {°F) T, = stack temperature (°F) T,1d = absolute temperature at standard conditions (528°R) Tt = Duration oftest run in minutes. Also see 8 Um = mean molecular speed (cm/s) Ym = sample volume (fe) at meter conditions Vm51d = volume standard (dscf), sample volume adjusted to 68°F and 29.92 inches Hg. V, = velocity of stack gas (fpm) y w = volume water vapor (set) at 68°F and 29.92 inches Hg. Wfwc = weight of the condensed water collected (grams) xd = fraction of dry gas Y = meter calibration Y-factor (dimensionless) II'= dimensionless inertial impaction parameter, O.I4 ,p. ... • .., .& General Sample Equations ? As= (05-I 4) • 1t 8"5 = Vw I (Vmstd +Vw) C8 =Me • 0.01543 I Vmstd Ccond = Mcond • 0.01543 I Vmstd Ccors = Mcors • 0.01543 I Vmstd Cra = Tstd • Crp • Ps • Xd I [Pstd • (Tm + 460)] Cr= Mrp • 0.01543 I Vmstd CPMIO = MPMIO • 0.01543 I Vmstd Crad = CuriesNmstd Cga1 (corr) = Cgas • (20.9-desired %02) I (20.9-actual %02) case Dpso = -,J [)..lS • \jJ • N • 1t • D/ • 18 I (Kc • Pp • Osee • 4)] PM,. Dp;o = 0.15625 • [(T5 + 460) I (Ms • P5)]0'2091 • ()..1.5 I Osc)0·7091 ERcond = Ccond • Os • 0.00857 ERcors = Ccors • Os • 0.00857 ERF = Cr • Os • 0.00857 6 ERK"·' = Pstd • Os • Mwgas • Cgas • 60 I (R • Tstd • I 0 ) ERgm = Cgas(lbldscf) • Os • 60 (Either ERgas equation gives equivalent lblhr values to 3 sig. figures) ERmmBtu = Cgas(lb/dscf) • Fd • (20.91(20.9-%02), Method 19 Equation 19-1 ERPMIO:::: CPMIO • Os • 0.00857 ERrad :::: Crad • Qs • 60 Kc:::: 1 + 2 • A. • 1.257 I Dpso A :::: Jls I (0.499 • Ps • U m) Md = C02 • 0.44 + 0 2 • 0.32 + N2 •0.28 Ms = (Md • Xd) +(I 8 • Bws) )..ls = [51.05 + 0.207 • (T5 + 460) + 3.24 •10'5 • (T5 + 460)2 + 0.53147 • %02-74.143 • Bwsl • 10'6 Ps:::: PbP +(Po 113.6) 8, = (-,JllP1' I -,JllP'ave) • (81est I pts) 8n:::: 8, • -,JllPn I...JllP1 Oa = Ys • As Qs = Qa • Xd • Ps • Tstd I [(Ts + 460) • P51d] Osc = [(Ts + 460) • Pstd I (Tstd • P5)] • [(Vmstd + V w) I 8] Osee = [(T5 + 460) • Pstd I (Tstd • P5)] • [(Vmstd + V w) I 8] Ow= QsiXd Ps = P5 • M5 • 3386.39 • 10-61 [R • (T5 + 460) I 1.8] Urn= 100 • -,J {[R • (T5 + 460) 11.8 • 8 • 103] I [1t • M5]} Vmstd = Vm • Y • Tstd • (Pbm + llH I 13.6) I [Pstd • (T m + 460)] V5 = 85.49 • 60 • Cp • -,Jflp • -,J [(T5 + 460) I (P5 • M5)] Yw= Wtwc•0.04715 Xd = 1 -Bws APPENDIXB South Yell ow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data Yellow Cake Dzyer Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data B South Yell ow Cake Dryer Scrubber Facility Energy Fuels . .. Stack Identification South Yellow Cake Dry_er Scrubber i A Date Barometric Pressure N Pbn, in Hg Pbp in Hg 8 Static Pressure (PG) in H:O Estimated Moisture (Bw,) 4-6% % Sample Height from Ground 70 feet Comments: Stack Dm 12.75 Rcterence 0 Pons arc 7' Upmeam from nc\t disturbance Pons are 30' DOIIllStream from last disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B I c D E F I 6.7 0.85 0.85 2 25.0 3.19 3.19 3 75.0 9.56 9.56 4 93.3 I 1.90 11.90 Averages: Ts ___ _ L. FlO\\ ---- C.P .Vt.P -------- KEY=> IM5: Field Data Sheet Plant:~ Date:~ Traverse II Time ---.- Point 1 1 1 2 2 2 3 3 3 4 4 4 1 1 1 2 2 2 3 3 3 4 4 4 Total , Avernge DGM Operator: __ -1----+-------- aP II aH (~H,OI II Vacuum II I Te~peratures :'F) I ~ DGMT~p (T,.) .J \]·-t,t.{O) " .sstt 3tp·'1 v [·~ \ <l 1.-~~o ID1·~ l(D :rs- Gs" <-t ·C1 Page _Lor-\-Run#_j_ r 8 0 N Slack Diameter 12. 75" Port Reference --"'0-" __ J ?:__Upstream from next disturbance 30' Downstream fll)m Jnst distut:bance Assumed Moisture _ 4-6 % .Probe -z """f). S Cp 0.84 NozzlcQllibml~on / ...,,---~ t....J.u -l-"t t:D . c..."+S AvgD. ~b -- Gas Bag If:-0 ::} Console_____}, Y-Foctor (-·C) 1.) c:_ aHa I . L f> in H20 Barometric Pressures Pbm "'2-'-/.. ]=~ in Hg PbP 2 '-( · ftJ<;r in Hg Pc -• 3 d) in H20 Leak Check: Pre Post L/- fl'imin (? .oD4 0 ·6D ( vocinHg 2} ( <: Pilol Rale 0 • U lnH,O UJ · S Water Collected Time Sampled Review a·D ~·~ i-{'Zt \ .lJ K= K= !!.C) @Tm @T,. g min t l 7 • ' I 4-'!' -' . I 5" --+J ~-'-'~\ ==--til v ..,~ u ~· -;---~ t-tl ~7~-.'-'~: 5::£, ~,f7/ I k-' I ..., '"{ 1'\ ) ~\ ., . ,~, ·"'''\" ,_q,t- 0· -DQ~ ).\p\~ I .. .. rn i__ Field Data Sheet TETCO 12. Filler {, { ( 1., Sample Box._.:._/ /_ Page L--or--\ Run~~~ ..,, Eni'~;r~~ Date: ""' Travene Point ... '· Operator: ---F:....-r DGM II t.H t;n HPt II Vacuum II I Te~peratures rn I ~ DOM T~p(T,.) 86 r N ~__! ~1 4~ ---=---! I J,'f(; ~I -• _v, " _'-G n: !!/, l 'r -~ 11-+---11 : _-n I KJ"' ' I ::=::t:..tJ..,:;' ?I > , IY. :. I ~<J 'i> ,,Stllek Diameter 12.75" Port Refercncc_,O_" __ ( 2 f.~ l.(b 2 z_ 3 ,o __ 3 tfll~ '3 4 ;-1~ 4 ~~·--4 = '{_1 tLJ 'IL.1 $"" 2 (p t-~ t0 4 ~~ 4 Total 3 q ~oe,'f7 .J 14-o\4~ .;-s~c{v t.toctlO { .1 01-( ot.\·s-- tAOl, <( ~ ~ . ..:, Ports arc 7' Upstream from next disturbance ~orts arc 30' Downstream from last disturbance Assumed Moistu_r; ~ 4-6 % Probe 1· t Cp 0.84 Ni1~Calib'i~ .1 t{ 1 t5 • _A_v_g_D" 1 W'~ in-ch_c_s - . --- Gas Bag~ Console__,.~.:__- y -Factor / ' l)b :Z: t.Hg /· ~ )CJ in H20 Barometric l'rtss~ Pbm zy.1~ in Hg l'bP li-~l6 inHg Pc ( 0 • / J in H20 Leok Cheek: Pre Post .-- R1/min 0 --:QD 1 o7oo 5 VIle in Hs '7 1... __2_Q Pilol Rllte Q . 0 D·o lnH,O ~·~ ~ Water Collected '-1~ &-· 5r Time Sampled~ Review K= K = @Tm @Tm . {ol"i" ) ,-.€6\~ z_.ou..s . lt \\ g min Yell ow Cake Dryer Baghouse ~. .. Prelim 6 pts i Facility Energy Fuels B Stack Identification South Yellow Cake Dryer Baghouse Date N Barometric Pressure A Pbm in Hg PbP in Hg Static Pressure (P0) in H20 Estimated Moisture (Bw5) 1 % Sample Height from Ground feet Comments: Stack Dia 16" Reference: 0 Ports are 57" I Upstream rrom next disturbance Ports are 454" iJ Downstream from last disturbance Time: Traverse Percent Distance From: Ports Point Diameter ID Reference A B c D E F 1 4.4 0.70 0.70 2 14.6 2.34 2.34 3 29.6 4.74 4.74 4 70.4 11.26 11.26 5 85.4 13.66 13.66 6 95.6 15.30 15.30 Averages: Ts LFiow -------- ~P ___ _ v~P __ _ KEY=> ~p L Flow! It '-{ Field Data Sheet ~ Plant: Denison Mines Date; I{ I f"f \~ Traverse Time Point Clock Min (9) 1 1o:-&1-0 2 !(0 3 120 4 }.Q 5 !.{€) 6 50 1 1t:o1 lc.o 2 ::w 3 80 4 qo 5 too 6 110 \'!l:ol \'Z.O Total A -·-.g- Commenls: Time tl \oo ~~~ 1}) l\~~01 TETCO Filter (,10""1-SampleBox_A __ OOM AP AH tnH,OI Vocuum (O'J (mHp, Desired 131 .l..o'1 .7C[ 1.9,--r 1'41.>. 'Z-~0 ·~lo 'l.o'-1. ISS. z~.( ·~.S '1,.~e h.~. 3")0 ·~tO -z..o~ 113.~~0 ·t"'t ·-z. .ot., IS Z. ·'-~0 ·t{ 2.01 t~l.l,.fy •93 z."l.o 1.c:>J.Of0 • ct-( '2:}$ 'l.lo. ~ {o • 'tc.( (..1.1. l'Z.0./'2..'0 .rJo IRO 21g.~tao I "6 I ,.~( 13':}-. s~a I "JCf I, "6).. l.<Ho • l.0J Lo~ , to'1-'1 '<./ ll· .l~~~ ./ " .q~ 1.1-' BaghouseAP Time ~.,. fl.~ol, s.v 11! tc:> ~ •• 1..-tt:~~ Actual f•1fl) t. 8+-'{ 'Z·()o.l 1( 'Z.·D8 ~ -z..o~ &.\ 1. .o{o 5 'Z.ol 5 z:z.o 5 '2. .'2,.;' s 1. •l.(.. s· l.'fo 5 1-~1 '{ '· 8+-t.( Zt(. '-{oo / l.o:, ~ BaghouseAP S.t. 5,"'1., s.t..-- Location: Yellowcake Dryer Baghousc Operator: M. · ~ ~ lJ [JJJ-tAl ,_ Temperatures m Stack (T,) Probe Probe: Out Filter ,-( 27:< Z'' •') z;'-{ 7{ 7.70 ~)\ 2-5'\ 15 210 Z..~.o; ?.:){ '1) l"Cf t<B l.fS ,_, 110 1'(~ "Z.£10 1-l "2.30 "?,..~{{ Zli-( '1(., 27o ~bl!) zc .. o l(o Z-ro 2.{8 Z.(.q 11 l,i;.o 'Z,.c.{"'{ l<H /7 2!S '2. 1" I ~-5'1 ll 1,S:( ~d"t{ ?..,4 ..,~ l'i( z f3 2-:'J ct tl / / l'J. ~1-- DGM Te:mp(i;., Effluent Out In 53 10 '-6 '1-{ '1-z.. c.."'( l.f-:r 1€> -,o "l't '?>0 1t s t ~1..-11.. 51. 4lN 11.. 'iCf Bo ?-; Lf1 gj "1'1 'ire B<f 1i ~~ 9A' )( 'i~ ~'? f':r 't~ ~ 7\? rt& ~ ll.~ ~ Loc;J,e,C-. -:r tJo..(feJS . i Page _\ of -Run# I_- B t ·0 N Stack Diameter _16" __ Port Reference _0.0"_ P/f arc ~T Upstream from next disturbance • POrts arc ¥.sy'~ Downstream from last disturbance Assumed Moisture • o/o Probe •13-b Cp~ Nozzle Calibration I "'2-'Z.."$ l l'2.3 I 2_2."3, ....J..3:?:2 Avg D. '2.'Z. ) inches Gas Bag Ambienl Air Console ---'91--- Y-Foctor I· 00 L. liH0 ~ •to) L-in H20 Barometric Pressures Pbm 24,71 inHg Pb• 2 Lf · f.. tQ in Hg Pq -l· ~ . in H20 l..ai:Chec:k: Pre 11'/min 0 00(.. \'lcinH~<..O· 0 PilocRaleo .o lnH,O t•O ~ O·Oo Z..,. n.o o.o "')A} Water Collected {., · ~ g Time Sampled ''2. 0 min Review ~ K• K- @Tm @T. -... "' South Yell ow Cake Scrubber Sample Recovery Gas Analysis Data (ORSA T) Yell ow Cake Dryer Baghouse Sample Recovery Gas Analysis Data (Ambient) Chain of Custody Lab Analysis APPENDIX C c South Yell ow Cake Dryer Scrubber .... METHODS Facility: Energy Fuels Stack Identification: SYC Scrubber Date: l(t<i / l 1 ----~-;__.!...._ ~~~~~------------------------- WJ!W{IEBS \ ~ ~ Run: Sample Box: ~ ·(o tOi '~ !0 C{ L? \ ro (ol I ( IMI!IJS{I~BS "II 2- IMPINGEBS Final (g) Initial (g) Net (g) 1 Run: 1 drop out I (., 7o ,{ t{"T=J-.3 I l:l3 1 "L Run: 1 drop out I Iiiipinger l"'um6er 2 I 3 I 4 I 5 6 Initial Volume.ofliquid (H20) in imp!ngcrs, (ml) 100 I droE out I 100 I Silica Gel Total (g) (J --- 1---Sample Box: 8 )m~inger l"'umlier 2 I 3 I 4 I 5 6 Initial Volume of liquid (H20) in impingcrs, (ml) 100 I drop out I 100 I Silica Gel I , • , • 813.2.. ~~1.5 ~q:l ·l. 5 Jv ·LJ 111'1C..· -:3 ~35-r s(,t)L/.O & f-IP· ¥ s-z.l ? ~~o.'l \(I . '-\ 31 .5" I~ ·'-l 8., (o)·'\ Total (g) tt9B.8 Sample Box: lmp10ger Number 2 I 3 I 4 I 5 6 Initial Volume of liqui<l(H20) in ·impingers; (ml) WO I drop out I 100 I Silica Gel , Final (g)------+-------+-------+------+-----+------- Initial (g)------+-------+------+------+------+------ Net (g) ======d=====~==================~====== Total (g) ---------~ --=-========= IMPINGERS Run: Sample Box: 1 2 Iiiipinger Number I 3 I 4 I s 6 Initial Volume ofliquid (H20) in impfngers, (ml) drop out 100 I drop out I 100 J Silica Gel I J Final (g) -------1-------+-----~------1------+----- Initial (g) ____ --+------+-----+------+-----1------- Net {g)==========::::b====:!:========::b:=== --~ ---------Total (g)::==~===::==: wr~ 1/1'~ I I~ _. -L' Plant t:: VI e.r" vI +--.~~ _) c::::. '.{ (_ Location ...; ·--------~----~--------------------Analytical Method ORSA T I[,,\.~ Average Actual Net Net Actual Net Net Date Gas Reading Volume Test No. Gas Bag No. C: -o 1-\. . \ \. l \. l Ambient Temp t! L \ I· I. Operator Date~ Average Actual Net Net Actual Net Net Gas Volume TestNo.~ Gas Bag No. .....o Ambient Temp · 2•0 Z·b 2•0 Z,o -z,o z.a Operator ·() Actual Net lr-------T-------~r------~----~r------~------41 Average Net Actual Actual Net Net Date Gas Volume -----Test No. ____ _ Gas Bag No. ____ _ Ambient Temp ____ _ Operator ____ _ CO is not me85ured, 85 it h85 the same molecular weight 85 N2 Yell ow Cake Dryer Baghouse ,tf ., .•. ~ f'l Method 5 Facility: Energy Fuels Date: ~~I ) /11 ______ __:_.....:.. Stack Identification: Yellow Cake Dryer Baghouse IMPINGERS l Filter Numb# ~2135" lolol IMPINGERS Filter Number IMPINGERS Filter Number Final (g) Initial (g) Net (g) Run: 1 100 I 5Cft.O (,/,.(o -2.7 .~ Run: l Sample Box: 2 lmfnger Number I 3 I 4 I s Initial Volume ofliquid.{H10) in impingers, (ml) 100 I I SilicaGel I 1 ' . ~14 ·11 c, I {. t/J'l t:t ~0. '-{. {011.~ v W.<t 9o~.6 1-PJ "f.~ Z.l ' & Total (g) =====~ ' Sample Box: lmpinger Number 2 I 3 I 4 I 5 Initial Volume ofliquid (H20) in impingers, (mi) 100 100 I I SilicaGet I 6 ~ 6 Final (g) ___ --t----+----+----+------11----- Initial (g) -----t----+-----+----+------11-----Net (g) ============~========================== Run: Sample Box: lmpmger Number ] 2 I 3 I 4 I 5 6 Initial Volume of liquid {H10) in impingers; (ml) 100 100 I I SiticaGel I Final (g) -----t----+-----+----+----lr---- Initial (g) ___ --t----+----+----+----lr---- Net (g) ============~========================== Total (g) ======= Chain of Custody Record Temperatura on Receipt ---Test America Drinking Water? Yes 0 NoD THE LEADER IN ENVIRONMENTAL TESTING TAL-4124 0!Xm Client Tetco ~· -P{Ofl!t:f ¥D!t89'J!f __ Dean Kitchert. .. _ .... . ..... Telephone Numb9r (Area Code )/Fax Numb6r 391 East 620 South 1801-492-9106 ~ -· . I Stato I Zip Code Site Contact · Amencan Fork Ut :_ 84003 I Lab Contact Proj4a Natmt and Location (StaiB) "' Energy Fuels 2014 1st Quarter ContracilPurchase Orrflllf/QuoiB No. Sample I.D. Na. and Description (ContslnetS for tMCh sample may be combined on one line} Date ' R1 Baghouse filter (6107) and beaker 01/15/14 "l- R1 SYC filters (6108, 09, 10, 11) and beaker 01/14/14 R2 SYC filters (6112,13,14, 15) and beaker 01/15/14 -. I ·L__---=--... ··--------- Scott Chrilt~nsen, Garren P•lmer I cariiei-twaybffl Nuiiibar Containers & PreseNatives Matrix Time ~~ ~~~~~~ I I i I ~ I ~ I ~ ~~~I n :oo :! X 8:00 X 8:00 X l 0 1;;. ::1 z. ' ::) i!: ·, -. • X., o I -, X I -' ., Date -+ 1/17/2014 ----1 LBb Number Analysis (Attach list ff more space is neBded) 0 ~ ;; .... "0 1:. ~· -, -. x, -.-- Chain of_ c~ [;prrper- Page or Special Instructions! CondffionsofRece~t Possible HBZBrd !denlilitlltloil ---,Sample D/$posiJ 0 Non-Hazard 0 Fltlmrnable 0 Skin kritatrl 0 Poison 8 0 Unknown 0 Rerum To Cllant 0 Disposal By Lab (A fee may be B6SIIISS6d if samples am retained 0 Arr:hive For ___ Months ~ lhml1 month) TumArOUndT(m~ 0 24 Hours ~ ~rs @{Days ..,0 14 Days 0 21 Days 0 ()ttJBJ; a~ per method 0C: Raqult!U719/ItS (Spedty} 1:-~~ NJ--fl-:_ ~r l,r_ ('{1!_-;,/;cf I /z 1. Rt~Cflivtld.By (lito (NM :t. fWt:alvtld By IDDI~r I~ S. RllCfiMtd By !Oatil 'Tmo 2.~~ -....-I'"" 'TifJlO 1 Date 3. R6JiriQ(Jl$hedB_y (~ ,Do~ Commllllts When Complete Email to: Dean or Paul tetco@tetco-ut.com DISTRIBUTION: WHITE :·Re!Uiiiiii:lto Client with Rej>ort; CANARY ~·Shlys Wfth-·ltle"'~Si""m""IP071e"';'P"'1N"'Kv--F""l"'el""CJ.,.C""op='y:------------------------------------ SDGNo. Ordct·No. 47741 TestAmerlca Inc l'piSTLRchTitle v3.73 Tes!America Laboratories, Inc. Analytical Data Pac){age Prepared For Denison Mines (USA) Corp. Energy Fuels 2014 1st Quarter Radiochemical Analysis By TestAmerica Inc 2800 G.W. Way, Richland Wa, 99354, (509)-375-3131. A.!isigned Laboratory Code: Data Package Contains 14 Pages Report No.: 58580 Results in this report relate only to the sample(s) analyzed. Client Sample ID (List Order) Lot-Sa No. Work Order Report DB lD R1 Baghouse J4A210418-1 M2WD61AA 9M2WD610 filter(61 07)and be R1 SYC J4A210418-2 M2WEQ1AA 9M2WEQ10 fllters(6108,09, 10,11)a R2SYC J4A210418-3 M2WET1AA 9M2WET10 filters(6112,13,14,15)a Batch No. 4023018 4023018 4023018 Test America THE LEADER IN ENVIRONMENTAL TESTING January 29, 2014 Denison Mines (USA) Corp 1050 17th Street, Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab Project Name Sample Type SDGNumber I. Introduction Certificate of Analysis January 21, 2014 Energy Fuels 2014 1st Quarter Three (3) Stack Filter Samples 47741 CASE NARRATIVE On January 21,2014, three stack filter samples were received at TestAmerica's Richland laboratory for radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification numbers as described on the cover page of the Analytical Data Package report form. The samples were assigned to Lot Numbers J4A210418. IT. Sample Receipt The samples were received in good condition and no anomalies were noted during check-in. ill. Analytical Results/Metbodology The analytical results for this report are presented by laboratory sample ID. Each set of data includes sample identification information; analytical results and the appropriate associated statistical uncertainties. The analysis requested was: Alpha Spectroscopy Uranium-234, -235, -238 by method RL-ALP-004 Tes!America Laboratories, Inc. 2 Denison Mines (USA) Corp January 29, 2014 IV. Quality Control -· The analytical result for each analysis performed includes a minimum of one laboratory control sample (LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments" section. V. Comments Alpha Spectroscopy Uranium-234. 235. 238 The achieved MDA of the batch exceeds the detection limit due to the reduced aliquot sizes taken due to historical process knowledge. Data is accepted. Except as noted; the LCS, batch blank and sample results are within acceptance limits. I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically and for completeness, for other than the conditions detailed above. The Laboratory Manager or a designee, as verified by the following signature has authorized release of the data contained in this hard copy data package. Reviewed and approved: TestAmerica Laboratories, Inc. 3 ....• ' Drinking Water Method Cross References .T --,--·· DRINKING WATER ASTM METHOD CROSS REFERENCES Referenced Method lsotope(s) Test:Amerlca Richland's SOP No.'-- EPA 901.1 Cs-134, 1-131 RL-GAM-001 EPA 900.0 Alpha & Beta RL-GPC-001 EPA 00-02 Gross Alpha (Coprecipltatlon) RL-GPC-002 EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002 EPA 903.1 Ra-226 RL-RA-001 EPA 904.0 Ra-228 RL-RA-001 EPA 905.0 Sr-89/90 RL-GPC-003 ASTM D5174 Uranium RL-KPA-003 EPA 906.0 Tritium RL-LSC-005 ___ .,. ·----·- ·---.. ~ Results in this report relate only to the sample(s) analyzed. Uncertainty Estimation TestAmorica Richland has adopted the internationally accepted approach to estimating uncertainties described in ''NIST Technical Note 1297, 1994 Edition". The approach, "Law of Propagation of Errors", involves the identification ofall variables in an analytical method which are used to derive a result. These variables are related to the analytical result (R) by some functional relationship, R =constants • f(x,y,z, ... ). The components (x,y,z) are evaluated to determine their contribution to the overall method uncertainty. The individual component uncertainties (uu are then combined using a statistical model that provides the most probable overall uncertainty value. All component uncertainties arc categorized as type A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the components, such as sample homogeneity, are combined with the component uncertainty as the square root of the sum-of-the-squares of the individual uncertainties. Tho uncertainty associated with the derived result is the combined uncertainty (uc) multiplied by the coverage factor (1,2, or 3). When three or more sample replicates are used to derive the analytical result, the type A uncertainty is the standard deviation of the mean value (S/?n), where Sis the standard deviation of the derived results. The type B uncertainties are all other random or non-random components that arc not included in the standard deviation. The derivation of the generai"Law of Propagation of Errors" equations and specific example are available on request. TestAmarlca lne ratGcncrallafo v3.72 TestAmerica Laboratories, Inc. 4 ------- ~- ·--· 1--- --· Action Lev Bntch Bias COCNo Count Error (#s) Total Uncert (#s) u. _ Comblued Uncertainty. (#s), Coverage Factor CRDL(RL) Lc Lot-Sample No MDCIMDA Primary Detector Ratio U-234/U-238 Rst/MDC RstrrotUcert Report DB No RER SDG Sum Rpt Alpha Spec Rst(s) Wori<Ordcr Yield Tes!Amerlca Inc rotGenct·allofo v3.7:Z TestAmerica Laboratories, Inc. Report Definitions _ An ngn.cd upon nt ti\llly love! used to trigger some 11ctlon when the Cimil result is greater than or equol to the Action Level. Often the Action Level Is relnted to the Decision Limit. The QC preparation balch number that relates laboratllry samples to QC sample's that were prepared and nnalyzed together. Defined by the equation (Result/Expected)-! as defined by ANSI Nl3.30. Chain of Custody Number assigned by the Client or TestAmeriCII. Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same units as the result For Liquid Scintillation Counting (LSC) the batch blank count is the background. All known uncertainties associated with the preparation and 1111alysis of the sample are propagated lo give a measure of the uncertainty associated with the result, Uc the combined uncer/alnty. The uncertainty is absolute and in the same units as the result The coveruge factor defines the width of the confidence interval, I, 2 or 3 standard d~viations. Contractual Required Detection Llmlt as defined in the Client's Stutement Of Work or TestAmerica "default" nominal detection limit. Ofien referred to the reporting level (RL) Decision Level based on inslrument background or blllllk, adjusted by the Efficiency, Chemical Yield, ami Volume associated with the sample. The Type I error probability is approximately 5%. Lc=(1.645 • Sqrt(2•(BkgmdCnt/BkgrndCntMin)/SCntMin)) • (ConvFct/(Efi*Yid•Abn•Vol) • Tngrl'ct). ror l.SC methods the batch blank is used as a measure oflhe background variability. Lc cannot be calculated when the background count is 7cro. The number assigned by the LIMS software to track samples received on the same day for a given client. The sample number is a sequential number assigned to each sample in the Lot Detection Level based 011 Instrument background or blank, adjusted by the Iifficlency, Chemical Yield, and Volume with a Type I and TT error probability of approximately 5%. MDC~ (4.6S • Sqrt((BkgrndCnt/BkgrndCntMin)ISCntMin) + 2.71/SCntMin) • (CunvFct/(Eff • Yld • Abn • Vol)' lngrFct). For LSC methods the bntch blank Is used as a measure of the background variability. The instrument identifier associated with the analysis of the sample aliquot. The U-234 result divided by the U-238 result The U-234/U-238 ratio for natural uranium in NIST SRM 432JC is 1.038. Ratio of the Result to the MDC. A value greater than I may indicate activity above background at a high level of confidence. Caution should be used when applying this factor and it should be used in concert with the quulifiers associated with the result Rntio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of2 a value greater than 1 may indicate activity above background at approximately the 95% level of confidence as~'Uming n two-sided confidence interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result Sample Identifier used by the report system. The number is based upon the first five digits of tl1e Work Order Number. The equution Replicate Error Ratio"' (S-D)/[sqrt(TPUs2 + TPUd2)] as defined by !CPT BOA where S is the original sample result, Dis the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the total uncertainty of the dupliCIIte sample. Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt. The ~urn of the reported alpha spec results for tests derived from the same sample excluding duplicate result where the results arc in the same units. The LIMS software assign test specific Identifier. The recovery of tha tmcer added tll the sample such as Pu-242 used to trace a Pu-239/40 method. 5 Report No. : 58580 Cllentld Batch Work Order Parameter 4023018 FFSR R1 Baghouse filter(6107)and be M2WD61AA U-234 U-235 U-238 R1 SYC filters(6108,09,10,11)a M2WEQ1AA U-234 U-235 U-238 R2 SYC filters(6112,13,14,15)a M2WET1AA U-234 U-2.35 U-238 No. of Results: 9 Sample Results Summary TestAmerica Inc Ordered by Method, Batch No., Client Sample ID. Result+· Uncertainty ( 2a) Qual Units 1.17E-03 +-2.6E-04 uCi/Sample 4.52E-05 +· 3.5E-05 uCI/Sample 1.27E-03 +-2.7E-04 uCi/Sample 1.08E-03 +-2.4E-04 uCi/Sample 3.45E-05 +-3.1E-06 u uCI/Sample 1.07E-03 +-2.4E-04 uCi/Sample 1.22E-03 +· 2.6E-04 uCifSample 1.85E·05 +· 2.4E-05 u uCIISample 9.73E-04 +· 2.2E-04 uCI/Sample Date: 29-Jan-14 SDG No: 47741 Tracer Yield MDL CRDL RER2 69% 4.04E-05 S.OOE-15 69% 2.63E-05 9.00E-15 69% 3.26E-05 S.OOE-15 77% 5.96E-05 S.OOE-15 77% 3.48E-05 9.00E-15 77% 5.30E-05 9.00E-15 81% 4.82.E-05 S.OOE-15 81% 4.19E-05 S.OOE-15 81% 4.07E-05 S.OOE-15 TestAmerlca Inc RERl ·Replicate Error Ratio • (S-D)I[sqrt(lq(TPUa)+sq(J'l'Ud))] aa denned by ICPT DOA. rptTALRchSaSum mary2 V6.2.26 A2002 U Qunl • AnRiyzed for but not cletccted above limiting crltcriR. Limit criteria Is less thaD the Mdc/Mdnfl\ofdl, Total Unccrt, CRDL, RDL Ol' not Identified by gamma .sun software. TestAmerica Laboratories, Inc. 6 Report No. : 58580 Batch Work Order Parameter FFSR 4023018 BLANK QC, M2WRQ1AA U-234 U-235 U-238 4023018 LCS, M2WRQ1AC U-234 U-238 No. of Results: 5 QC Results Summary TestAmcrica Inc Ordered by Method, Batch No, QC Type,. Result-t· Uncertainly ( 2e) Qual Unit& 1.09E-07 +-2.2E-07 u uCUSample -2.43E-08 +-1.5E-07 u uCUSample -6.98E-08 +-1.6E-07 u uCUSample 7.37E-06 +-1.8E-06 uCUSample 7.41E-06 +-1.8E·06 uCI/Sample TestAmerlca Inc Diu • (ResuiUF.xpceletl)-1 ns defined by ANSI N13.30. Date: 29-Jan-14 SDG No.: 47741 Tracer LCS Yield Recovery Bias MDL 75% 4.69E-07 75% 4.05E-07 76% 6.94E-07 71% 98% 0.0 3.32E-07 71% 95% -0.1 3.91 E-07 rptSTLRchQcSum U Qunl -Annlyzed for but not detected a hove lhnltlng criteria. Limit criteria is Ius thMn the MdrJMdn/Mdl, Total Uncert, CRDL, RDL or mary V&.2.26 notltlenllfletl by gammn scan soOwue. A2002 TestAmerica Laboratories, Inc. 7 -! CD (/) ); 3 CD :::1. g r "' cr 0 ~ 0 :::1. CD _rn 5" p GD Lab Name: TestAmerlcalnc Lot-sample No.: J4A210418-1 Client Sample ID: R1 Baghouse filter(6107)and be FORM I SAMPLE RESULTS SDG: 47741 Report No. : 58580 COC No.: Date: 29-Jan-14 Collection Date: 1/15/201411:00:00 AM Received Date: 1/21/2014 11:55:00 AM Matrix: FILTER Energy Fuels 2014 1st_Qu~rter _ _ _ _ __ Ordered by Client Sample 10, Batch No. Result Count Total MDL, RptUnlt, Yleld Rst/MDL, Analysis, Total Sa Aliquot Primary Parameter Qual Error( 2&) Uncert(2 s) Action lev lc CRDL(Rl) Rst/TotUcert Prep Date Size Size Detector Batch: 4023018 FFSR Work Order. M2WD61AA Report DB ID: 9M2WD610 U-234 1.17E-03 1.8E-04 2.6E-04 4.04E-05 uCVSample 69% (29.) 1/28/14 06:48 p 1.0 0.00129 ALP2 1.10E-05 9.00E-15 (9.1) Sample Sample U-235 4.52E-05 3.5E-05 3.5E-05 2.63E-05 uCi/Sample 69% (1.7) 1/28/14 06:48 p 1.0 0.00129 ALP2 6.11E-06 9.00E-15 (2.6) Sample Sample U-238 1.27E-03 1.8E-04 2.7E-04 3.26E-05 uCi/Sample 69% (38.8) 1/28/14 06:48 p 1.0 0.00129 ALP2 8.19E-06 9.00E-15 (9.3) Sample Sample RaUo U-2~8 -0.9 No. of Results: 3 Comments: TestAmerlca Inc MDCIMDA,lc-Detllctlon, Decision Laval based on Instrument background or blank, adjustlld by the sample Efficiency, Yleld, and Volume. rptSTLRchSample U Qual -Analyzed for but not detectlld above limiting criteria. llmlt criteria ls less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not Identified by gamma scan software. V5.2.26 A2002 .. a;t "' > 3 Ill :::!. lil r IP C" Q ... 0 :::1. Ill !." :; f' CD Lab Name: TestAmerica Inc Lot-Sample No.: J4A210418-2 Client Sample ID: R1 SYC filters(6108,09,10,11)a FORM I SAMPLE RESULTS SDG: 47741 Report No. : 58580 COCNo.: Date: 29-Jan-14 Collection Date: 1114/2014 8:00:00 AM Received Date: 1/21/2014 11:55:00 AM Matrix: FILTER Energy_fuels 2014 1st Q!JC!rtf:!r Ordered by Client Sample ID, Batch No. Result Count Total MDL, Rpt Unit, Yield Rst/MDL, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL.(RL) Rst/TotUcert Prep Date Size Size Detector Batch: 4023018 FFSR Work Order: M2WEQ1M Report DB 10: 9M2WE010 U-234 1.08E-03 1.6E-04 2.4E-04 5.96E-05 uCi/Sample n% (18.1) 1/28/14 06:48 p 1.0 0.00124 ALP3 1.81E-05 9.00E-15 (9.1) Sample Sample U-235 3.45E-05 u 3.0E-05 3.1E-05 3.48E-05 uCI/Samp!e n% 0.99 1/28/14 06:48 p 1.0 0.00124 ALP3 9.16E-06 9.00E-15 (2.2) Sample Sample U-238 1.07E-03 1.6E-04 2.4E-04 5.30E-05 uCi/Sample n% (20.2) 1/28/14 06:48 p 1.0 0.00124 ALP3 1.57E-05 9.00E-15 (9.1) Sample Sample Ratio U-2341238 = 1.0 No. of Results: 3 Comments: TestAmerlca Inc MDCIMDA,Lc-Detection, Decision Level based on Instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Lindt cr1ter1a Is less than the Mck:/Mda/Mdl, Total Uncart, CRDL, RDL or not Identified by gamma scan softwaro. V5.2.26 A2002 , • ;;;t "' 5> 3 (1) :::1. !il r-QJ c:r 0 iil 0 :::1. (1) !" 5" fl ...... 0 Lab Name: TestAmerica Inc Lot-Sample No.: J4A210418-3 Client Sample ID: R2 SYC fllters(6112,13,14,15}a FORM I SAMPLE RESULTS SDG: 47741 Report No. : 58580 CCC No.: Date: 29-Jan-14 Collection Date: 1/15/2014 8:00:00 AM Received Date: 1/21/201411:55:00 AM Matrix: FILTER Energy Fuels 2014 1~t Quarter _ _ _ _ Ordered by Client Sample 10. Batch No. Result Count Total MDL, RptUnft, Yield Rst/MOL, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2s) Uncert(2 s] ktion Lev Lc CRDL(RL) Rst/TotUcert Prep Data Size Size Detector Batch: 4023018 FFSR Work Order. M2WET1AA Report DB ID: 9M2WET10 U-234 1.22E-03 1.7E-04 2.6E-04 4.82E-05 uCi/Sample 81% (25.3) 1128114 06:49 p 1.0 0.00128 ALP4 1.41E-05 9.00E-15 (9.4) Sample Sample U-235 1.85E-05 u 2.4E-05 2.4E-05 4.19E-05 uCVSample 81% 0.44 1128/14 06:49 p 1.0 0.00128 ALP4 1.18E-05 9.00E-15 (1.5) Sample Sample U-238 9.73E-04 1.5E-04 2.2E-04 4.07E-05 uCi/Sample 81% {23.9) 1128114 06:49 p 1.0 0.00128 ALP4 1.14E-05 9.00E-15 (9.) Sample Sample Ratio U-2341238 = 1.3 No. of Results: 3 Comments: TestAmertca Inc MDCJMDA,Lc • Detection, Decision Level based on Instrument background or blank, adjusted by tho sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual ·Analyzed for but not detected abova limiting criteria. Limit criteria Is less than the MdciMda/Mdl, Total Uncert, CRDL, RDL or not Identified by gamma scan software. V5.2.26 A2002 . ., • -1 CD "' s; 3 CD g· r ... c::r 0 iil 0 :::>. CD !." 5" p ..... ..... Lab Name: TestArnericalnc Matrix: FILTER Count Parameter Result Qual Error (2 s) Batch: 4023018 FFSR U-234 1.09E-07 u 2.2E-07 U-235 -2.43E-08 u 1.5E-07 U-238 -6.98E-08 u 1.6E-07 No. of Results: 3 Comments: Total MDL., Uncert(2 s) Lc FORM II BLANK RESULTS RptUnlt, CRDL Yield Rst/MDL, Rst!T ottJcert Work Order: M2WRQ1AA Report DB 10: M2WRQ1AB 2.2E-07 4.69E-07 uCi/Sample 75% 0.23 1.27E-07 9.00E-15 (1.) 1.5E-07 4.05E-07 uCi!Sample 75% -0.06 1.04E-07 9.00E-15 -0.32 1.6E-07 6.94E-07 uCI/Sample 75% -0.1 2.09E-07 S.OOE-15 -0.86 Ratio U-2341238 = -1.6 SDG: 4n41 Report No.: 58580 Analysis, Total Sa Prep Date Size 1/28/14 06:49 p 1.0 Sample 1/28/14 06:49 p 1.0 Sample 1/28/14 06:49 p 1.0 Sample TestAmerica Inc MDC(MDA,lc-Detection, Decision Level based on Instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. Date: 29-Jan-14 Aliquot Primary Size Detector 0.1 ALPS Sample 0.1 ALPS Sample 0.1 ALPS Sample rptSTLRchBiank U Qual-ADalyud for but not detected above limlling criteria. Limit criteria Is Jess than the MddMda/Mcll, Total Uncut, CRDL, RDL or not identified by gaiiiiiUI scan software. V5.2.26 A2002 • ~ "' ~ 3 !!! i:i" r Dl C" 0 iil 0 ::I. Ill !" 5" p ~ "' Lab Name: TestAmerica Inc Matrix: FILTER Count Total Parameter Result Qual Error ( 2 s) Uncert(2 s) MDL FORM II LCS RESULTS SDG: 47741 Report No. : 58580 Report Unit Erpected Recovery, Yield Expectro Uneert Bias Analysis, Prep Date Batch: 4023018 U-234 FFSR Work Order: M2WRQ1AC Report DB ID: M2WRQ1CS 7.37E-06 1.3E-06 1.8E-06 3.32E-07 uCi/Sample 71% 7.49E-06 2.31E-07 98% 1/28/14 06:49 p RecLimlts: 70 130 0.0 U-238 7.41E-06 1.3E-06 1.8E-06 3.91 E-07 uCI/Sample 71% 7.84E-06 2.42E-07 95% 1/28/14 06:49 p RecLimlts: 70 130 -0.1 No. of Results: 2 Comments: TestAmerlca Inc Bias -(ResllltiE:s:pected)-lAS defined by ANSI NI3.30. rptSTLRchLcs V5.2.26 A2002 Date: 29-Jan-14 Aliquot Size 0.13 Sample 0.13 Sample Primary Detector ALPS ALPS ·-· -·-····--··--- mt ~ 3 CD :::1. g r "' CT 0 iil 8" :::1. CD !!' 5" " .... c.> .. Chain of Custody Record TAIA1a4 (llllm Temperature on Receipt --- Drinking Water? YesO ·NoD Test America THE LEADER IN ENVIRONMENTAL TESTING c:rlotJt. " -/'rDjtlct MlltZglr .. -- -- ---lfua i Tetco _ __I ! De<!.fl._Ki~n _ _ ------= ~=------; r iliiizo14 ~ • -----• ---T~.Fil (Mill~~ ,L.to~ 1391East 620South ~-492.9~----·--I ~ I ~~Siltf4 Z1P c.-. &1a Ci>n:u.J: Ub ~ Amll}'sfs (A11Bch list If l !~eri;a_!!Fork ---' Ut-~84003 l..,.:;;;.w..;~:....,_;._.--~~ 1'-~.-IS~ :~~~ct;;;.;;,,:-=---:__:_=~-1 ~ I I J i J . ~ · . eontamer.; & J MaiJVr PI'BSfJrvatives ~ 10! ;:ll ~ I.D. No. and DMctfp"on I i I ~ a ~ ~· ~. :;11 iJ ~foreach~mayl»coml>lnedarotrfiiiM) Dale Tune :1! l ;J ~ -:1! ~ =11 l ~ S! FvJ.=i=... j Rl Baghouse filter (6107) and beaker 01/15/14 u:OO: XJ X· •j ' ! Rl SYC filters 16101,09, 10, lll and beaker ; 01/14/14 8:00: rx I ! X ·::o ~ IR2 SYC filters (6112. 13.14, 15) and beaker I ! 01/15/14 [a:oo , Xl · 7 l ;.~ c=-~1\1~ Willi\\ \\\\\II\ l\1 1,---1 I ~ --4 10418 J I I --I ~ . .. -:s~ ~ -a Vu'·~.v:.f ' ~ -'-V'V\"-\' ~~ d-\~-\'-\ ,C;!.:ioof~~ - P#ga of ~ Special lnstructtonsl Conditions of Receipt ~ 0. \.A..)\::)~ \'V\~~ '{Y\'a\..0~ ~~~tm ~~....,~~ D (A'"" maybll~ if samples""' retained o~ D F18mtn8b1r D Sl<in ,_ D PrMm B -D lkll<nawn D -7b Cllllnt 0 D/llpOuJ By w ~For ___ ~"'-'~ 7llm~'Bno.~ cc:~ (Sp«tfy} 0 24Houts ~Houts rl7a-0 14aq, 021Days D Otllet[as.uer metbod_ Uidr~bW/:;;Lz,C)~ ~ L lir.ld..rln; ~ 1.~8/ JOB (me v.-.C:t.~. -:5.~-rflt-ut.-'~a ,_,L\ \ \SS. Z.~B.)! lvar. l»n<t 2.~ I~ ln. 3. . ..,. 8y Ia. Inn. 3.-...tO)o ln."' lli?:c -CCiUilbot< . When Complete Email to: Dean or Paul tetco@teb:,:::o-;;:u~.t~.co=.i:m,:.,...,,.,.,==->=,...=~=------...!.' --------------------------Dirmf~Bqntilf:>9Htrt:-=-Ffiiiimiili0d;.ntii#h~ ~IWIY · .511ys w~~~~·fl':<l SiiiiiP10ii P1r1K • Rer:~CiY>Y' TestAmerica Sample Check-in List THE LEACER IN I!HVIRON ... INTAl TE8TIN~ ~ \ Date!fime Received:-----1..::--=....:. V\_!._-_,\'-'-\-\--t----'\u.\S........_S~-Container GM Screen Result: (Airlock) ~cpm Initial~t-;; Sample GM Screen Result (Sample Receiving) ~cpm Initials~ Client.: ~f;10 SDG #: \.....\II\ Y'\"-\ \ SAF -#:, ___________ . LotNumbc:r: =:S'U.-~ d,Y\:::>'·-\\'( ChainofC1.1stodyff. _________________________ --------- Shipping Container ID or Air Bill Number : NA ~ ] Samples received inside :;hipping container/cooler/box Yes\-, ] Continue with 1 through 4. Initial appropriate response. No Q ] Go to 5, add comment to #16. 1. Custody Seals on shipping container intact? Yes [ ] No [ No C\lslody So~~ ] 2. Custody Seals dated and signed? Yes [ J No [ No ~:tody Seal \~ J 3. Cooler tempenmrre: oc NA r ] 4. Vermiculiteipaoking materials is ~ Wet [ ) Dry [ ) 5. ChainofCwit<>dy rccprd presenl7 Yes ] No [ Item 5 through 16 for SR!llples. lnitinlappropriate response. ~ 6. Nnruber of samples received (Ei\ch Gatnpla llUIY contain mul spit bottles):_,....__--=----------- 7. Containers receive(\:~. t' ~ ·1 ~ i-'cAAY...u · 8. 9. 10. 11. 12. 13. 14. 15. 16. Yes [ ; No~ ] __ custody seals ~~p;jprlnte sample labels __ S (Air, Niosh 74bQ) ~T (Biological, Ni-63) es: Sample holding times exceeded? NA [ Samples have: ___ tape __ hazard labels Matrix: __ A (FLT, Wipe, Solid, Soil) __ I (Water) are in good condition · __ are leaking __ are broken __ have air bubbles (Only for samples requiring no head space) __ Oth~ Sample pH appropriate for analysis requested Yes [ ] No [ ] NA ] (If acidification is necessary go to pH area & documllnt sample lD, initial pH, amount t 0) added and pH after addition on table) Were any anomalies identified in sample receipt? k Yes [ ] No 'r ) Description of anomalies (include sample numbers): NA Ll ] ------------------ Sample Location, Sample Collector Listed on COC? "' •For documentation only. No corrective action needed. Yes [ ) No~'?] Additional InformRtlon:4~'----------------------------- T ] Client/Courier denied temperature check. ] Client/Courier unpack cooler. Sample Chec-k-i Signature: ___ , ~~~"""~~~:::_ ___ . ______ Date: \·d..\-l'j Dnte: By: \/, Person contacted: [ .\J No nction necessary; process ~is . _ _J Project 'Mllnngcr 2. A ~ ~'-------"-1_-..... ?"""-""2'----I_L-.J--/- LS-023 Rev. 17,05/13 Page 1 ofl TeslAmerica Laboratories, Inc. :• .. APPENDIXD South Yellow Cake Scrubber Figure 1. Facility Schematic Representation Yell ow Cake Dryer Baghouse Figure 2. Facility Schematic Representation Process Data (Retained by Energy Fuels Resources) D Facmty: Energy Fuels Resources t CL t y Stack Identification: South yell ow Cake Scrubber 1~0~1 J3 a: Distance upstream from next disturbance, feet ---- ~: Distance downstream from last disturbance, feet y: Distance of Sample Level to Ground, feet - 0: Stack Inside Diameter, inches . - Estimated Moisture, percent Estimated Velocity, fpm _-_· ·'-~----- Control Unit Type: Scrubber Number of Ports Figure I. Facility Schematic Representation Process Type: Yell ow Cake Processing • Facility: Energy Fuels Resources t ex t ). y Stack Identification: yellow Cake Dryer Baghouse 1~0 -+-I 13 ex: Distance upstream from next disturbance, inches 57" ~: Distance downstream from last disturbance, inches 454" y: Distance of Sample Level to Ground, feet 65' 0: Stack Inside Diameter, inches ~ Estimated Moisture, percent 0-2% Estimated Temperature, °F 125 Estimated Velocity, fpm I ,400 Control Unit Type: Baghouse Number of Ports 2 oE Figure 2. Facility Schematic Representation Process Type: Yellow Cake Processing ·. , ' .. .. •./.\ .. '' :i ~-~··" !r Energy Fuels Resources, Blanding, UT Process Data Source: South Yellow Cake loate: 1 J,v_f,l! Scrubber Flow GPM 4 c~y..trv Time #1 #2 ilP ~:;,o t>'.o 1..:-{· ~ /u·1- to.' o o 1 s~ u (..,'-'t•e:} {0·1- tv: so \c.\ ~'-t-"1 (v·-4 l(.'oo l~.V Z£1·<6 /D. :f l/.' J 0 t '.I l~·1 ,u.~ tz·.oo I~-I z "''~ r o .-::; {t~3l> l c;-,\ 2'-{ ., ( 0 ·-=1 l) :o 0 \ 5'. \ 24-l·ti /0·"'::/. t > .' 3 o f} ,'Z.. 24·~ Jl)•-=l l 4 ~ .:JD I~ .. ') '2'-{~ I o .'-f \ L( : ~D ,(·-~ '2. '-\ ~ I b 1- tr: o o 1)·---f 'Z-fr'1 {c-+ tS:~o ~~.) zLf.~ fD·-:J- f(p.' 00 15·) z~.~ ( 6 ·-:! /f?.' ,)0 /~·1-Z'i ·1 ( C:Y 1 f 1 : aD /(p·Z. 2.-"t .j (c·'1- r:J ... 3 o { (R ·t 2-'-< ·1-(t~.--1 I tr.. C)l> 1G·t. ~·~·~ Jc .1----' rr-:7u l(p-f..., -zu -1-1 o·-t' Energy Fuels Resources, Blanding, UT Process Data Source: South Yellow Cake Date: J1s,i_ Scrubber Flow GPM c~,.,.. fc...J.-r I} ..... ~ Time #1 #2 ~p }. : (.) i) ''1·¥' "Z'f· '1 VD. :+ b-_· 10 tLi·'i 2 Lf. ·f I lJ ·1- '1.: 0 0 pJ• s 2 '-1·1 ( {) ·+- 4.: 3 ~ 1'1·'1 2 L(, i ro·t- to.'c.Jc Jt..f·~ z l.( • y { ().-;} /O.'Jo I b · ( 2 '-(, '1 ( o·1 /(: (.) 0 \ ~·> -z_~·U ( 0·1 l( ,• S D IS ·<1 2 v('') t o·1 IZ~.::>D l~·r;-'7 ~· () (0·-+ tZ.') o f~. t, z S"· 0 L o ·1 I J: o D /5". ~ 2(;.0 I 0 ·1-{'~;e>D 1'$.' "$0 liP. 0 ztf. 4 t0·1- ('-{.' 0 j) l& ,-z_, 25-.0 (6.-:j It{: 3 o I lP . c..( 2.(. 6 ( () . t (5: oo I~·~ 2'-l· I lo·.:.? r~: 3 o {(,. ~ 't {., (D·:} tv: i)o { (, . ) t').D /0·1 /6 : 56 lG ·~ v1.v ro·t' I J APPENDIXE Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature sensors were carried out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 3 Schematic of Method 5/114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-test Dry Gas Meter Calibration Data Forms Type S Pitot Tube Inspection Data Sample Box Temperature Sensor Calibration E Temperature Sensor t ~Probe TypeS Pitot Tube Temperature sensor lrqqerTrain Q:llional, M!r;'BeRepaced 8f hi EqUvalert Condenser l Temperature Sensor Te~~~~re Gooseneck Nozzle j H:lliltTr.mf "" ~ / R'Obe ~-------------- lmpingers -~ / TypeS Pitot Tube ~ Stack Wall Glass Filter Holder Heated Area Manometer Temperature Sensors Orifice Air-Tight Pump Figure 3 Schematic of Method 5/114 Sampling Train Vacuum Gauge METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES y bhiiG@IIQ0@d@iii!h 1) Select three critical orifices to calibrate the dry gas meter \\tlich bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. ENVIRONMENTAL SUPPLY COMPANY 3) Run attested vacuum (from OrifiCe Calibration Report), for a period of lime necessary to achieve a minimum total volume or 5 cubic feet. 4) Record data and information in lhe GREEN cells, YELLOW cells are calculated. DATE::) ·~~"',..._ I METER SERIAL ,,1522588 I CRmCAL ORIFICE SET SERIAL ~: 1oi63S EQUIPMENT ID II: G G G RUN I 2 3 2 3 2 K' TESTED FACTOR I VACUUM (AVG) (In Hg) 0.8137 13 951.176 G.l1l7 13 963.468 0.8137 13 9611.784 0.5317 12 941.2114 0.5317 12 946.l&D 0.6317 12 951.636 0.3~? 13 975.015 0.3~7 1l 980.846 0.3307 13 916.447 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 963.4CI 9!i8,7a4 974.125 946.360 951.536 957.031 980.1146 986.447 992.040 5.293 5.316 5.341 5.156 5.176 U9S 5.130 5.602 5.593 76 71 75 7<& 75 76 66 66 65 67 66 61 75 76 75 74 75 73 74 76. 71 67 68 70 74 73 73 77 ao ao 11 13 83 73 71 71 70 ' 70 75 78 74 74 74 74 74 DGM AVG 76.5 77.5 79.75 69.26 69.00 70.15 75.50 73.75 73.50 Facility FINAL I 25-40 I ELAPSED TIME(MIN) a AVG (P,.,) 25.4 §§90 2.90 2.90 §§.20 1.20 1.20 13.50 13.00 13.00 New Calibration 2013 ~ 4.£12 .!.mi 4,3827 ~ ~ ~ .!:!.1.n 4.71151 IF Y VARIATION EXCEEDS 2.110%, ORIFICE SHOULD BE RECALIBRATED ~ 4.4691 ~ AVG• ~ ~ 4.71i7 AVG• 4.9040 4.7224 Yill AVG: ~ !,!!!!!! .Y!! l.!!!!2 l,!!!J2 l:J!!!! ~ 1.009 ~ ~ ~ 1.003 1 :Ml ~ ::!!:!!!. The following equations are used ID calculate lhe standard volumes of air passed through lhe DGM, V m (sld), and lhe critical orifiCe, V. (sld}, and lhe DGM calibration factor. Y. These equalions are aulomalicaHy calculated in !he srreadshee! above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = [JJW{] (1) (2) (3) Vm,,.,,, = K, • f·'m • Pbnr+!,l!.H /13 6) Tm Vc.·r 1 .. .,,~ = K '• = Net volume of gas sample passed through DGM, corrected to standard condrtions K, = 17.64 'Rim. Hg (English), 0.3858 'Kimm Hg (Melric) T.., = Absolute DGM avg. temperature ("R • English. 'K -Mel ric) = Volume or gas sample passed through the critical orifice, corrected to standard conditions T-= Absolute ambient temperature ('R-English, 'K-Meine) K' = Average K' factor tram Critical Orifoce Calibration rc'i .. llll Y= -J"1n,,.,,,J = DGM calibration factor AVERAGE 6.Ha =I 1Ji5Q 2 6.He = ( 0.75 9 ) .<l.H (Vm{std)\ v.,(sld) v.. J Temperature Sensors Reference In Out "F 33 67 202 "F 34 68 203 "F 34 68 203 !:ill 1.717 .1:Zl!! .till l.ill ~ .1&!!! .!ill j,ill METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES -:S-.. ;, 1) Select three cntical orifices to calibrate the dry gas meter wh1ch bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run attested vacuum (from Onfice Calibration Report). for a penod of \1me necessary to achieve a mmimum total volume of 5 cubic feet. 4) Record data and mformat1on m the cells. YELLOW cells are calculated. METER SERIAL ll:j.....:=:..:.::::=~ CRITICAL ORIFICE SET SERIAL II:.._ _ __;;...__, EQUIPMENT ID II: K' TESTED .----.----l FACTOR I VACUUM I I RUN II I IAVG) (In Hg} 0 G G 2 3 2 3 2 J 0.8137 12 0.8137 12 0.8137 12 0.5317 12 0.5317 12 0.5317 12 O.JJ07 12 0.3307 12 0.3307 12 88.612 94.007 99.387 105.106 110.310 115.878 121.205 126.327 131.458 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 94.007 5.395 65 78 99.387 5.380 65 79 104.803 5.416 ~ 79 110.310 5.204 m 75 115.878 5.568 m n 121.084 5.206 m n 126.327 5.122 72 76 131.458 5.131 72 76 137.053 5.595 72 76 79 75 79 75 80 ~ n " n n ~ n 76 71 76 72 76 72 75 75 75 n n n 72 72 72 DGM AVG 76.75 71.00 77.25 72.75 74.00 75.00 73.75 74.00 74.00 FINAL ,-25.45 J ELAPSED TlME(MIN) 8 5.00 5.00 5.00 7.50 8.00 7.50 12.00 12.00 13.00 ENVIRONMENTAL SUPPLY COMPANY AVG tp,.,) 25.45 3.00 3.00 3.00 1.20 1.20 1.20 § 44 44 2014 Pre-Calibration Console 9 ~ ~ 4.5676 4.4031 ~ ~ ~ 4.3217 4,7125 IF Y VARIATION EXCEEDS 2.00',(,, ORIFICE SHOULD BE RECALIBRATED l ~ !!.!ru. ~ 0.996 4.5203 ~ AVG= 0.993 ~.96 4.4097 1.,.W ~ 1.001 4.4097 1.005 AVG= ~ !1m ~ !,Q1i 4.380 .till 4,7450 L.QQ! AVG= 1.012 !1.2! The following equations are used to calculate the standard volumes of air passed through the DGM, V m (std), and the critical orifice, v. (std). and the DGM calibration factor. Y. These equatiOns are automatically calculated 1n the spreadsheet above. AVERAGE DRY GAs METER CALIBRATION FAcToR, Y = Qooi I (1) (2) (3) I·,,.,,, ~ 1\ I • I'm• !'hell'+ (Mill J 6) 1iu I#Lr _A:' l'har • (:-) ,,,. .. J l'anlh = Net volume of gas sample passed through DGM, corrected to standard condi\1ons K, = 17 64 "Riin, Hg !English) 0 3858 "Kimm Hg IIVIetroc) T m = Absolute DGM avg. temperature ("R-English, "K -IVIetroc) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T ~• = Absolute ambient temperature ("R -English "K -IVIetroc) K' = Average K' factor from Crollcal Onfrce Cahbratran _l'cr!_~ -,~, •• M• = DGM cahbratron factor AVERAGE li.He =( 1.652 I 2 £\.HI!!!= ( 0.75 B ) Ll.H (Vm(std)) V.,(stdl Vm Temperature Sensors Reference In Out •F 32 72 201 •F 33 73 202 •F 33 73 203 .1.lli !,ill 1.741 !,ill 1.648 1.,lli .1lli 1.565 ~ Console 9 Pre-test 2014 . . .I METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES ~ !ifflii!tDifi ... RM<fi@·'m·-=: iii! -......... ---- 1 1) Select three crrtical onfices lo calrbrate the dry gas meter whrch bracket lhe expected operaling range 2) Record barometric pressure before and after calibrallon procedure ENVIRONMENTAL SUPPLY COMPANY 0 0 G 3) Run at tested vacuum (from Onlice Cahbratron Report), for a period or lrme necessary to achreve a minimum total volume of 5 cubrc feet 4) Record data and rnlonnation rn the cells, YELLOW cells are calculated METER SERIAL #:I ·-----I CRITICAL ORIFICE SET SERIAL U:1 ·----1 EQUIPMENT 10 #: K' TESTED FACTOR !VACUUM RU;;, (AVG) (In Hg) 2 J 2 3 2 3 0.8137 0.8137 0.8137 0.5317 0.5317 0.5317 0.3307 0.3307 0.3307 13 13 13 12 12 12 13 13 13 § 141.101 148.155 148.165 154.241 164.241 159.683 § .0 .D .0 7.054 6.086 5.442 .0 .D .0 I ll 1-l I 75 57 65 63 72 76 65 70 72 77 76 70 c__]!__ 77 78 ~-- Fl-1111 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: DGM AVG 0 0.00 64.25 71.00 75.50 0.00 0.00 0.00 Facility ~ AVG(P.,,) I zs.8o I 25.80 ELAPSED TIME {MIN) 0 §§ § 0 20 10.50 9.00 8.00 §§ Energy Fuels 6.1483 6.Z371 ~ IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED l AVG= 6.2291 1.013 ~ !.ill 4.7460 1.022 AVG= 1.018 ~ AVG= The loliolwlg equa110ns are used lo calculate lhe standard volumes of ar passed through lhe OGM, V~ (sld). and lhe critical ortftee, V0 (Sid). and lhe DGM cabbfalion faclor Y These equalions are automatically calculaled rn the Sjl(eadsheet above AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = r-1.018 ] (1) (2) (3) I"m,.,,,, "J.:,•l"m• f'har+( \11113 6) ]-.~~--~~ J l 'I",HI, J..·•,. l'h11r • (-) ,_;,,,,, " Net volume or gas sample passed through DGM, corrected to standard condrtions K1 = 17 64 °R/tn Hg (English), 0 31158 "KKmm Hg (Metric) T m = Absolute DGM avg temperature (0R -English. "K -Metric) = Volume or gas sample passed through the critical orifice corrected to standard conditions T,mo = Absolute ambtenl temperature ("R-English "K-Meine) K' = Average K' factor !rom Crihcal Onlice Cahbrahon l"n ;,l-1, = DGM cahbrahon factor l"m,.:.ll AVERAGE ~HI!!=[ -a5rJ ~HII! = ( 0.75 0 )2 dH (Vm(std)) Vc1(std) Vm Temperature Sensors Reference In Out "F 33 67 202 "F 34 68 203 "F 34 68 203 1.672 1.650 !,ill Type S Pitot Tube Inspection Oat<~ Date _____.::\_?..,__( I_Z.,__{ :..=11_ Pttot Tube ldcntilicauon __ ..:.1....;€;>:.._-_(].:::_ _____ _ .. C< Tcchnic tan ,.,. Dt= ·3"'t-) Ill r. = .... ,~(.. In rs = . '-1 '1 L In [tl < 10" a,= • ((1<100 u!= ,0 p, < 5" B I = __ ,;.2=---- Pl= ___ 2 __ _ Z $0 125 in Z = _..;.•_o_:o:...~.:._ __ in. ·Y ~ =------... w w .. -+ __.....~-·--·~-- W :S 0 03125 in w = __ . o_o__:e __ m W > J mches w = __ ....;(.._._)_-__ In Z > 3/4 inch Z= ______ m I I r t:, ., •. ,. ..•. . · ··{ ·:~ 1]-··-• -~-----y ~ 3 inche.s Y = __ 3_, _.(' __ .... m The pilot tube meets the spccilications for a calibration factor of0.84? 'I~ ~ Tcmpt'rn!Urc Sensor CnlihmiiO'.::n:_.. _____ _ Reference :J ~df Temperature Tcm ncrature Tompcrntnn:: Source Reference Sensor Dit1crence ~::{·· :;Ji-< (Medium) (''f) ("f) t·"F> AIR /2.. lL 0 Probe Continuity '(e. s Heat Check 248 y~s L{O AIR 71.. lz.. 0 ICE WATER 33 1y [ Stack BOIL WATER Z-ol. 2.o L 0 SILICONE OIL £ 1 ypc ~ l'tlol J ubc Inspection Data Dat~ . Ptt~t Tube ldrntificntion: ___ 'l_;__:f.!.--_-____.:{;1~---- ... Dt= ·'1 "=1 ~ 10 r ..... ·~52. In Is P A = P !l ? _ _.'{'-~:;::.:~::...._ ____ _ Is L05 • D1 !> 01 !> 1.50 • D, ? __ '{.._-e..-=--~----- Pa = . <i) 2... In q, < 10" CLt = 0 CJ.1 < 10° al = {) r11 <.so ~~=------· z ]~ z~ o 125m .oH, Z= Ill ~ ~ ~~w -~ -·--· -· --~~ W ,; 0.03125 in. W= •ooB m ~-\V > 3 IIICh~S \V= 1-In ,., ... -""" .... ·@-E-}.:mJ ___ ~, Z > 314 inch Z= In / Y= 3, l The pi tot tube meets the specifications for a cahbralion factor ofO.R-P ~-· Stack Tcltt(!Cll\hue ScnsorC:~hht~uon Temperatur~ Source (Medium) AIR Continuitv Heat Check 248 AIR ICE WATER BOIL WATER SILICONE OIL Reference Sensor ("f) ("f) "2.50 2o3 Tclllpcratllt~ Dtffcrence (qF) TETCO Sample Box Temperature Sensor Calibration Dare: 12/13113 Cal ibraror. Dean Kitchen Rel;:rcncc: Ome~a CL3512A Thermocouple Temperature Temperature Temperature Unit ID Source Reference Sensor Difference Location (:\ledium) ("F) ("F) ("F) Water .,., 34 2 Oven .J_ Water 204 203 -I A Oven (4) Water 33 34 I Water 204 202 -2 lmpinger Out Water 33 34 I Water 204 203 -I Oven Water 33 33 0 Water 204 202 -2 B Oven (4) Water 33 34 I Water 203 203 0 lmpinger Out Water 32 33 I Water 204 202 -2 Water 32 .,., I Oven .J.J Water 204 203 -I c Oven (4) Water 33 34 I Water 204 204 0 Water .,., .,., 0 lmpinger Out .J.J .J.J Water 203 202 -I Oven Water 33 34 I Water 203 203 0 D Water .,., 34 I Oven (4) .J.J Water 204 204 0 Water .,., 33 0 lmpinger Out .J.J Water 204 202 -2 Oven Water 33 34 I Water 203 202 -I E Oven (4) Water 33 33 0 Water 204 203 -I Water .,., 34 I lmpinger Out .J.J Water 204 203 -I Oven Water 33 34 I Water 204 202 -2 F Oven (4) Water 33 34 I Water 204 202 -2 ' lmpinger Out Water 33 33 0 Water 203 202 -I Water .,., 34 I lmpinger Out G .J.J Water 204 203 -1 Impinger Out H Water 33 34 I Water 204 202 -2 Water 33 .,., 0 lmpinger Out I .).J . Water 204 202 -2 Water ..,., 34 I Jmpinger Out J .J:) Water 203 202 -I APPENDIX F The testing followed the same procedures as outlined in previous protocols and tests at this facility. Prepared for: Energy Fuels Resources 6425 S Hwy 91 Blanding, Utah 84511 Date of Report: August 27, 2014 SECOND QUARTER RADIONUCLIDE EMISSIONS TEST CONDUCTED AT ENERGYFUELSRESOURCES SOUTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE GRIZZLY BAGHOUSE BLANDING, UTAH June 16-18, 2014 by: TETCO 391 East 620 South American Fork, UT 84003 Phone (801) 492-9106 Fax (801) 492-9107 fax • CERTIFICATION OF REPORT INTEGRITY Technical Emissions Testing Company (TETCO) certifies that this report represents the truth as well as can be derived by the methods employed. Every effort was made to obtain accurate and representative data and to comply with procedures set forth in the Federal Register. Dean Kitchen R vi.e\1 er: ______ _,c,/&~· .:::..e:z_c'---~--'-==-- Date: _______ __,tf"~:).-.__6_-....:..../_t.f.:..____ jj TABLE OF CONTENTS PAGE Introduction Test Purpose ................................................. , ........... 1 Test Location and Type of Process ........................................... 1 Test Dates ........................................................... , ... 1 Pollutants Tested and Methods Applied. . ..................................... 1 Test Participants .......................................................... 2 Deviations From EPA Methods .............................................. 2 Quality Assurance. . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . ........... 2 Summary of Results Emission Results ......................................................... 3 Process Data ............................................................. 3 Description of Collected Samples ................................ , ..... , ..... 3 Discussion of Errors or Irregularities .......................................... 4 Percent Isokinetics ........................................................ 4 Source Operation Process Control Devices Operation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ............. 5 Process Representativeness ................................................. 5 Sampling and Analysis Procedures Sampling Port Location .................................................... 6 Sampling Point Location ................................................... 6 Sampling Train Description ................................................. 7 Sampling and Analytical Procedures .......................................... 7 Quality Assurance ......................................................... 7 Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence Ill Table I II ill N v VI Figure LIST OF TABLES PAGE Measured Radionuclide Emissions ........................................... 3 Percent Isokinetics ......................................................... 4 Sampling Point Location ................................................... 6 Complete Results, South Yell ow Cake Scrubber ....................... Appendix A Complete Results, Yell ow Cake Dryer Baghouse ....................... Appendix A Complete Results, Grizzly Baghouse. . .............................. Appendix A LIST OF FIGURES 1 Facility Schematic Representation South Yellow Cake Scrubber. .......... Appendix D 2 Facility Schematic Representation Yellow Cake Dryer Baghouse .......... Appendix D 3 Facility Schematic Representation Grizzly Baghouse .................... Appendix D 4 Schematic ofMethod 5/114 Sampling Train ........................... Appendix E iv INTRODUCTION Test Purpose This test project was conducted to determine the total radionuclide emissions from the South Yell ow Cake Scrubber, Yell ow Cake Dryer Baghouse, and Grizzly Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dsct). These tests were for U-Nat and Th-230 on the Grizzly Baghouse and U-Nat, Th-230, Ra-226, and Pb-210 on the South Yellow Cake Scrubber and Yellow Cake Dryer Baghouse. Test Location and Type of Process Energy Fuels Resources is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Dryer Baghouse. The Packaging enclosure also discharges into the Dryer Baghouse. The South Yellow Cake (NYC) dryer was the only operating dryer at the time of the test. The North Yellow Cake Dryer was not operating at the time of the test. The Grizzly Baghouse serve as the main dust control device for the raw ore unloading and conveying to the processing building. Stack schematics are shown as Figures 1 though 3 in Appendix D. Test Dates The first test run on the SYC Scrubber commenced the afternoon of June 16, 2014 and was completed the following morning. The second run started June 17t, 2014 and was completed the morning ofJune 18,2014. One test run was completed on the Yellow Cake Dryer Baghouse June 17, 2014. One run was completed on the GrizzlyBaghouse June 18,2014. Pollutants Tested and Methods Applied The tests were a determination of radio nuclide emissions in accordance with EPA Method 5/114. Test run filters and front wash residues were sent to Test America located in Richland, Washington for radionuclide analysis. Test Participants Test Facility State Agency TETCO Garrin Palmer None Doug Olsen Jeff Graton Deviations From EPA Methods None Quality Assurance Mike MeN amara Testing procedures and sample recovery techniques were according to those outlined in the Federal Register and the Quality Assurance Handbook for Air Pollution Measurement Systems. 2 SUMMARY OF RESULTS Emission Results Table I presents the findings of the test in pi co Curies per dry standard cubic foot and pounds per hour. Tables IV-VI in Appendix A have more detailed information. Grizzly Baghouse 1 2 0.06 AVE 25.4 Process Data The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow, pressure drop readings (~p) were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (~p) were recorded and are found on the test run sheets. Production data is retrained by Energy Fuels Resources. Description of Collected Samples The test filters for the South Yell ow Cake Scrubber were heavily covered with an off-white colored particulate. The front washes were clear in appearance. The test filters for the Yellow Cake Dryer Baghouse were lightly colored with a tan colored particulate. The front wash was clear in appearance. The test filters for the Grizzly Baghouse were had no visible particulate. The front wash was clear m appearance. 3 Discussion of Errors or Irregularities None. Percent lsokinetic Sampling Each of the tests were isokinetic within the ±10% of 100% criterion specified in the Federal Register. They also meet the Utah State Department of Environmental Quality, Division of Air Quality specification of isokinetic sampling point by point. !so kinetic values for each test run are presented in Table II. Run# 1 2 South Yell ow Yell ow Cake Cake Scrubber Dryer Baghouse 101 98 I 100 Grizzly Baghou e 97 -------- 4 SOURCE OPERATIO Process Control Devices Operation All process control devices were operated normally. Recorded scrubber water flow, pressure and baghouse ~p readings were recorded and are found on the test run sheets or in Appendix D. Process Representativeness The facility was operated normally. Production data was retained by Energy Fuels Resources. 5 SAMPLING AND ANALYSIS PROCEDURES Sampling Port Location The inside diameter of the South Yellow Cake Scrubber stack is 12.75 inches. The two, four-inch diameter sample port are located 28.24 diameters (30 feet) downstream from the last disturbance and 6.59 diameters (7 feet) upstream from the next disturbance. Figure 1 in Appendix Dis a schematic of the stack. The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch diameter sample ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 2 in Appendix D. The inside diameter of the Grizzly Baghouse stack is 18.75 inches. There are two, three-inch diameter sample ports located 2.56 diameters (48 inches) downstream from the last disturbance and 1.31 diameters (24.5 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 3 in Appendix D. Sampling Point Location Table III shows the distance of each sampling point from the inside wall according to EPA Method 1. Each point is marked and identified with a wrapping of glass tape and numbered. These points are determined by measuring the distance from the inside wall. Sample Point 2 3 4 5 6 7 8 9 10 11 12 NYC Scrubber 0.85 0.70 0.50 3.19 9.56 11.90 6 2.34 4.74 11.26 1.26 2.21 3.32 4.69 6.68 12.08 14.06 15.43 16.54 17.48 18.25 Sampling Train Description To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-51114 were followed. All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent interference of the sampled gas and particulate. The stack analyzers used to conduct Methods 1-5/114 are constructed to meet the specifications outlined in the CFR. The temperature sensors are K-type thermocouples. Heater, vacuum and pi tot line connections have been designed to be interchangeable with all units used by the tester. A 316 stainless steel probe liner was used for the tests. Figure 4 in Appendix E is a sketch of the Methods 5/114 sampling train. Sample boxes were prepared for testing by following the prescribed procedures outlined in Methods 5/114. Sampling and Analytical Procedures All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 5/114. Quality Assurance All equipment set-up, sampling procedures, sample recovery and equipment calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbook for Air Pollution Measurement Systems. 7 APPENDIX A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence 8 APPENDIX A Table IV Complete Results, South Yell ow Cake Scrubber Table V Complete Results, Yellow Cake Dryer Baghouse Table VI Complete Results, Grizzly Baghouse Nomenclature Sample Equations A TABLE IV SYC Scrubber COMPLETE RESULTS Energy Fuels CORPORATION, BLANDING, UTAH SOUTH YELLOWCAKE SCRUBBER EXHAUST Symbol DescriEtion Dimensions Run #1 Run#2 Date 6/16,17/2014 6/17,18/2014 Filter# 6206 6208 Begin Time Test Began 13:53 13:14 End Time Test Ended 12:09 12:22 Pbm Meter Barometric Presswe In, Hg. Abs 24.30 24.30 dH Orifice Pressure Drop In H20 1.103 1.066 y Meter Calibration Y Factor dimensionless 1.000 1.000 Vm Volwne Gas Sampled--Meter Conditions cf 343.714 337.542 Tm Avg Meter Temperature of 76.9 76.2 ;/M Sq Root Velocity Head Root ln. H20 0.5060 0.4998 Wt_.c Weight Water Collected Grams 434.1 433.1 Tt Duration of Test Minutes 480 480 cp Pilot Tube Coefficient Dimensionless 0.84 0.84 Dn Nozzle Diameter Inches 0.2745 0.2745 C02 Volume %Carbon Dioxide Percent 2.00 1.20 Oz Volwne% Oxygen Percent 17.50 18.70 N 2 &CO Volume% Nitrogen and Carbon Monoxide Percent 80.50 80.10 Vmstd Volwne Gas Sampled (Standard) dscf 275.442 270.819 Vw Volwne Water Vapor scf 20.468 20.421 Bws (measured) fraction H20 in Stack Gas (Measured) Fraction 0.069 0.070 Bw, (saturated) fraction H20 in Stack Gas (Saturated) Fraction 0.118 0.114 Bw, Fraction H20 in Stack Gas * Fraction 0.069 0.070 xd Fraction of Dry Gas Fraction 0.931 0.930 Mct Molecular Wt Dry Gas lb/Jbmol 29.02 28.94 M, Molecular Wt. Stack Gas lbllbmol 28.26 28.17 %1 Percent Isokinetic Percent 100.9 100.2 AVG T, Avg Stack Temperature OF 113.2 112.0 112.6 A, Stack Cross Sectional Area Sq Ft. 0.887 0.887 PG Stack Static Pressure In H20 -0.280 -0.280 PbP Sample Port Barometric Pressure ln. Hg. Abs 24.23 24.23 Ps Stack Pressure ln. Hg. Abs 24.209 24.209 Q, Stack Gas Volumetric Flow Rate (Std) dscfin 1.23E+03 l.21E+03 1.22E+03 Oa Stack Gas Volumetric Flow Rate (Actual) cfin 1.77E+03 1.75E+03 1.76E+03 Ys Velocity of Stack Gas fjJm 2.00E+03 1.97E+03 1.98E+03 Curies Radionuclides per sample pCi 13957.4 17.3 Crad Concentration ofRadionuclides pCi/dscf 50.673 0.064 25.368 ERr ad Emission Rate ofRadionuclides pCilbr 3.734E+06 4.646E+03 1.869E+06 * If the measured moisture content is greater than the saturated moisture level (supersaturated), the saturated moisture value will be used in all calculations (40 CFR 60, Method 4, Section 12.1. 7), Dryer Bag house 13 TABLEV COMPLETE RESULTS, PM Energy Fuels CORPORATION, BLANDING, UTAH YELLOW CAKE DRYER BAGHOUSE Symbol DescriEtion Dimensions Run #1 Date Date 6/17/2014 Filter# 6207 Begin Time Test Began 14:00 End Time Test Ended 16:04 Pbm Meter Barometric Pressure In, Hg. Abs 2430 ~H Orifice Pressure Drop In. H20 1344 y Meter Calibration Y Factor dimensionless 1.002 Vm Volwne Gas Sampled--Meter Conditions cf 89.030 Tm Avg Meter Temperature OF 84.3 >/M Sq Root Velocity Head Rootln H20 0.7690 Wtwc Weight Water Collected Grams 6.1 Tt Duration of Test Minutes 120 cp Pilot Tube Coefficient Dimensionless 0.84 Dn Nozzle Diameter Inches 0.2220 C02 Volwne% Carbon Dioxide Percent 0.00 02 Volwne% Oxygen Percent 20.90 N 2 &CO Volume% Nitrogen and Carbon Monoxide Percent 79.10 Ymstd Volume Gas Sampled (Standard) dscf 70.568 Vw Volwne Water Vapor scf 0.288 Bws Fraction H20 in Stack Gas Fraction 0.004 xd Fraction of Dry Gas Fraction 0.996 Md Molecular Wt. Dry Gas Jb/lbmol 28.84 Ms Molecular Wt. Stack Gas lb/lbmol 28.79 %1 Percent Isokinetic Percent 97.6 T. Avg Stack Temperature OF 107.1 As Stack Cross Sectional Area Sq. Ft. 1.396 Po Stack Static Pressure In. H20 -0.24 PbP Sample Port Barometric Pressure In. Hg. Abs 24.23 ps Stack Pressure In Hg. Abs 24.212 Qs Stack Gas Volwnetric Flow Rate (Std) dscfin 3.13E+03 Qa Stack Gas Volwnetric Flow Rate (Actual) cfin 4.17E+03 Ys Velocity of Stack Gas fi>m 2.99E+03 Curies Radionuclides per sample pCi 1693.8 Crad Concentration ofRadionuclides pCildscf 24.0021 ERr ad Emission Rate ofRadionuclides pCitbr 4.508E+06 Grizzly (2) TABLE VI COMPLETE RESULTS, PM DENISON MINES CORPORATION GRIZZLY BAGHOUSE Symbol DescriEtion Dimensions Run#1 Date Date 6118/2014 Filter# 6210 Begin Time Test Began 8:13 End Time Test Ended 16:21 Pbm Meter Barometric Pressure ln. Hg Abs 24.30 Mf Orifice Pressure Drop In H20 1.837 y Meter Calibration Y Factor dimensionless 1.002 Vm Volume Gas Sampled--Meter Conditions cf 416.247 Tm Avg Meter Temperature "F 84.9 .,ff'l.p Sq Root Velocity Head Root ln. H20 0.2595 Wt_.c Weight Water Collected Grams 12.9 Tt Duration of Test Minutes 480 cp Pita! Tube Coefficient Dimensionless 0.84 Dn Nozzle Diameter Inches 0.4088 C02 Volume% Carbon Dioxide Percent 0.00 Oz Volume% Oxygen Percent 20.90 N 2 &CO Volume% Nitrogen and Carbon Monoxide Percent 79.10 Vmstd Volume Gas Sampled (Standard) dscf 330.057 Vw V olwne Water Vapor scf 0.608 Bws Fraction H20 in Stack Gas Fraction 0.002 xd Fraction of Dry Gas Fraction 0.998 Md Molecular Wt. Dry Gas lb/lbmol 28.84 Ms Molecular Wt Stack Gas lb/lbmol 28.82 %1 Percent Jsokinetic Percent 97.2 Ts Avg Stack Temperature "F 82.7 As Stack Cross Sectional Area Sq Ft 1.917 Pa Stack Static Pressure In H20 -0.056 PbP Sample Port Barometric Pressure In. Hg. Abs 24.27 Ps Stack Pressure In_ Hg. Abs 24.266 Qs Stack Gas Volwnetric Flow Rate (Std) dscfin 1.49E+03 Q. Stack Gas Volwnetric Flow Rate (Actual) cfin 1.89E+03 vs Velocity of Stack Gas tpm 9.85E+02 Curies Radionuclides per sample pCi 103.7 Crad Concentration of Radionuclides pCi/dscf 0.3142 ERr ad Emission Rate ofRadionuclides pCi!br 2.804E+04 APPENDIXB South Yell ow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Field Data Sheet Yell ow Cake Dryer Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Field Field Data Grizzly Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Field Field Data B s = fraction ofwater in stack gas (may have designation of"measured" or "saturated") "measured" represents measured moisture based upon sample volume and water collected "saturated" is a calculated value based upon stack pressure and temperature ) = average of initial and final system zero gas calibration bias checks (ppm, percent) average gas concentration (as measured) 3 = concentration of particulate matter, back half (gr/dscf,lb/dscf, etc.) i = concentration of condensibles (grain/dscf) concentration of coarse particulate (gr/dscf) measured concentration of a calibration gas when introduced in direct calibration mode concentration of particulate matter, front half, actual stack flow (gr /act) concentration of particulate matter, front half (gr/dscf,lb/dscf, etc.) Cavg corrected for initial and final system bias checks (Equation 7E-5) average of initial and final system upscale gas calibration bias checks (ppm, percent) actual concentration of upscale calibration gas 1 = concentration of metals (ppm, J..lg/fe, etc.) atomic symbol replaces "metal" ~ = percent carbon dioxide in the stack gas pitot tube coefficient (0.84) ) = concentration of PM10 particulate (gr/dscf) i = concentration of radionuclides (pCi/dscf) ; = measured concentration of a calibration gas when introduced in system calibration mode -= Any species symbol may replace X. Units may be expressed as ppm, lb/dscf, etc. ) = actual gas concentration corrected to required percent 0 2 ; = Measured radionuclides per sample. Units may be pCi or uCi. ; = jet diameter (em) ~=Dioxins and Furans (See laboratory report for D/F descriptions and nomenclacture) [ = orifice pressure drop (inches H20) l = orifice pressure (inches H20) 1 = orifice pressure head (inches H20) needed for impactor flow rate nozzle diameter (inches) > = stack flow pressure differential (inches H20) ) = 50% effective cutoff diameter of particle (em) diameter of the stack (feet) , = percent excess air l = emission rate of back half particulate (lb/hr) i = emission rate of condensibles (lb/hr) emission rate of coarse particulate (lb/hr) emission rate of front half particulate (lb/hr) emission rate of a gas (lb/hr) emission rate per mmBtu of fuel ) = emission rate ofPM10 particulate (lb/hr) i = emission rate of radionuclides (pCi/hr) -= emission rate of compound which replaces X. Units are usually in lb/hr. > = Dry based fuel factor. Ratio ofthe gas volume of the products of combustion to the heat content See 40 CFR 60, Appendix A, Method 19, Table 19-2 for fuel factor values. Cunningham slip correction factor mean free path of molecules in gas phase (em) 1 = million Btu 1 = million Btu , -mass of particulate matter in probe and front wash (mg) ) -mass ofPM10 particulate (milligrams) molecular weight of stack gas, wet basis (lb/lbmol) c-mass of species "X". Units may vary and other descriptive subscripts may apply. gas viscosity (poise) molecular weight of gas species (g/gmol) I= number of jets per plate 2 = percent nitrogen in the stack gas 2 = percent oxygen in the stack gas > = average of the square roots of l'lP (may also be referred to as ASL'lP) 1 = square root of l'lP at point 1 of the current test, Method 201A '-square root of l'lP at point 1 of the previous traverse, Method 201A average of the square roots of l'lP from the previous traverse, Method 201A n absolute barometric pressure at the dry gas meter (inches Hg) absolute barometric pressure at the sample location (inches Hg) 1 -stack static pressure (inches H20) absolute stack pressure (inches Hg) j = absolute pressure at standard conditions (29.92 inches Hg.) ) = time of test (minutes) t = sample time (duration in minutes) at first sample point for Method 201A sample time (duration in minutes) at sample point "n" for Method 201A st = target test time for Method 201 A (minutes) stack gas volumetric flow rate (acfm) stack gas volumetric flow rate (dscfm) actual gas flow rate through the cyclone (acfm) actual gas flow rate through the impactor (acfm) 1 -wet stack gas std. volumetric flow (ft3/min, wscfm) ~ = gas constant (21.85 inches Hg*ft3/(lbmol*R)) particle density (1 g/cm3) stack gas density (g/cm3) stack temperature (°F) stack temperature CF) j = absolute temperature at standard conditions (528°R) t = Duration of test run in minutes. Also see 8 mean molecular speed ( cm/s) 1 = sample volume (ft3) at meter conditions j-volume standard (dscf), sample volume adjusted to 68°F and 29.92 inches Hg. velocity of stack gas (fpm) volume water vapor (set) at 68°F and 29.92 inches Hg. weight of the condensed water collected (grams) j = fraction of dry gas meter calibration Y-factor (dimensionless) 1 = dimensionless inertial impaction parameter, 0.14 General Sample Equations %1 = Vmstct • (Ts + 460) • 1039 I (8 • Vs • Ps • Xct • Dn2) As= (Ds2 I 4) • 1t Bws = Yw I (Vmstd +Vw) C8 = M8 • 0.01543 I Vmstd Ccand = Mcand • 0.01543 I Vmstd Ccars =Mears • 0.01543 I Vmstd Cra = Tstd • ClP • Ps • Xd I [Pstd • (T m + 460)] Cr= MlP • 0.01543 I Vmstd CPMIO = MPMJO • 0.01543 I Vmstd Crad = CuriesiVmstd Cgas (carr)= Cgas • (20.9-desired %02) I (20.9 -actual %02) case DPso = --J [J.LS • \jl" N • 7t • D/ • 18 I (Kc • Pp • Qsce • 4)] I 0.2091 0 7091 PM10 DPso = 0.15625 • [(T5 + 460) (Ms • P5)] • (J-L5 I Qsc) EReanct = Ccond • Qs • 0.00857 ERears = Ccars • Qs • 0.00857 ERF = Cr • Qs • 0.00857 6 ERgas = Pstd 0 Qs • Mwgas • Cgas • 60 I (R 0 Tstd • 10) ERgas = Cgas(lb/dscf) • Qs • 60 (Either ERgas equation gives equivalent lblhr values to 3 sig. figures) ERmmBtu = Cgas(Ib/dscf) • Fd • (20.91(20.9-%02), Method 19 Equation 19-1 ERPMIO = CPMIO • Qs • 0.00857 ERrad = Crad • Qs • 60 Kc = 1 + 2 • A • 1.257 I Dp5o A= J-Ls I (0.499 • Ps • Urn) Md = C02 • 0.44 + 02 • 0.32 + N2 •0.28 Ms = (Md • Xd) + (18 • Bws) J..ls = [51.05 + 0.207 • (T5 + 460) + 3.24 •10-5 • (T5 + 460)2 + 0.53147 • %02-74.143 • Bws] • 10-6 Ps = PbP + (PG I 13.6) 81 = (--Jl'iP1' I --Jl'iP'ave) • (81est I pts) en = el • .YL1P n I .Y!'iP I Qa = Ys • As Qs = Qa • Xd • Ps • Tstd I [(Ts + 460) • Pstd] Qsc = [(T5 + 460) • Pstd I (Tstd • P5)] • [(Vmstd + Yw) I 8] Qsce = [(T5 + 460) • Pstd I (Tstd • P5)] • [(Vmstd + Yw) I 8] Qw= QsiXd Ps = Ps • Ms • 3386.39 • 10-6 I [R • (Ts + 460) I 1.8] Urn= 100 • --J {[R • (T5 + 460) I 1.8 • 8 • 103] I [1t • M5]} Vmstd = Vm • Y • Tstd • (Pbm + L\H I 13.6) I [Pstd • (T m + 460)] Vs = 85.49 • 60 • Cp • --J!'iP • --J [(Ts + 460) I (Ps • M5)] Yw = Wtwc 0 0.04715 Xd = 1-Bws South Yell ow Cake Dryer Scrubber Facility Energy Fuels Stack Identification South Yellow Cake Dryer Scrubber r A Date Darornetric Pressure N Pb01 in Hg PbP in Hg B Static Pressure (P0 ) inHp Estimated Moisture (Bw,) 4-6% ~~ Sample Height from Ground 70 feet Comments: I• Stack Dia 12.75 Reference: 0 Po1 ts are 7' Upstream from next disturbance Ports are 30' Downstream from las\ disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B c D E F ' 1 6.7 0.85 0.85 2 25.0 3.19 3.19 , 75.0 9.56 9.56 .J 4 93.3 11.90 11.90 .. - Averages: Ts L. Flow ---- i\.P Vi\.P --------- L. Flow! ~p . KEY=> ~ ~ '? Field Data Sheet \Q TETCO r Fil!er&ZD Sample Box C 4- Plant: Energy F!lels • \ Date: <tl l(v (t\J{ {p L1-\ty{ Location: Souti;r"'(ellow Cake Dryer Scrubber Operator: "' ' Traverse 11 Ti~e II DGM Tonp (T .J Clock I Min {!l) II c•'> II ''" HP> I Out I In c.P DGM Pomt 1 1 1 2 2 2 3 3· 3 4 4 4 1 1 1 2 2 2 3 3 3 4 4 4 Total Avmsge i?,'-7)1 o 11~\''-\--500 lr-z.}d"l[TI\1-\~'Z.-nf'/ ~ t(,_o l1JR~ 1~2V ]'Z.-7l l s-11!1-¥:11~ C£0 ~~~-W-tr{J]-z~] f. v_Z) I l· u'il:?ll \l i? I "l§fll--s7t& )8j _ _Loj,ll;:tl2~-;f.> tDv 112.:rQ.&tl{][.J-~llt-(~]~[ If~ I -z-Ctzt-z.'?:OI--2--~~u rrf:-L:l -=tcs- 11. o I~D~s-o_][_-J{ )fTu'"'fL l·dc.~~ll!w I ZC;z_lz1s-l1. 3~T&3~r7I I 1 tv\ o 11 wl~-~ >rl .1-~ 1r 1-o--f I t·u1 1r-Z?JI 1 ~o I zvviZ--t, 1 I '2.. ~or=~ ?l ?il 1-f5 \~U II[P'7Z-·'72Vl1 -2--~1r [-o~l (~ o~][ 5 ILIJ'1 I wz_[ l~~T 1-s='11Sb--ll 1-&1 -::t-1 \ ((O llf_p..{!P.1-z"t41.1-1JlJ·lS".I J-~~~-~II'TI~!Zs-:3fl'-{PI z. )rl 5'~ II 1~ s-o .k I~ Gv .Jiu {; I . 'l-{Z-!1. t --:1-lrl· t s T1:-I 5lr51Jt-vD I -t1') I1-5YT t 7 TI 6) II _7-fl 9-~ 1, 7.-~ If" r~._{~ (.p J-z. Lt II H\_ 1'-:11 lr-~JI l \ Ct lzs \ 1~?-z:..Tz' \I 5"'o II rt I ~\ '¥.:D'1 11-~v l[ &~'1-~vr II. 1-~ 11-.,~ --, ·"~ ~ 1~11 i os 11. ') 7:1 z 30T2 > t I u. Lf J[ 3-_ol_7_0 ~ 1,o0 1113 1 :soolf~ ~r I\.\~ IRII \\ -~T'l~:Z:,IZ:-N TZtf?if~Tll 1li czr r ~~\{~-~z_~LITJ~r l[./c/ICLJI 1D( 1~\_u ~~~z~r~ll 7 ~1 y ~ ~ ~D_._<TV~TlL l-\-t..-ISJ tt/fL.--;5 ~~I 1'"1{ ~ 'ti-O ~ "-~" 0 111-:t~. x-"1?1[ -is-r TO?-[ (. 0 y /!Til ll D I Zl/'/ r-z>s-=rz3b I (p 'l ll +& I ~0 "74:~ I~·IMl~ II{. r c. I r.t c. /Ia! 1o ~ I ~031 '2 3~1 -z ~s-=~r 0~-r--=r=-lr <K-D ~~~'"1-Joo:J[~/ I·IZ It· !7 /~I ros-[-z..u.7 [ ~ 3Sf"Z3&I ~0 if'~~ I ~D ~~o ll~lS!" ~ c;~o11 -2_ ~~ ~s 1-.~ c.,JI-z;--_]IJolt IZ:'z:l [ 1-_Z_"L[-'Z 7~1-'~7 l ~I ~ o ,xu\.0 lr<6"~1.~ U.~l . z.=l Ill-v 2Ll·o~'Jf---.-01Lro~ D'f'ZTZ. ~srrz3 ~I ~ t II :4-C.., 1 go ~~o 11 %'-flP ·1¥111-z c,+-11 f·o~ IT·D~~] c;-][ i o?j ~'PIT~~T T Z.7vl e:~ II -:;.&I b--o rZ:o~ I.>...I&D-11~&/. 2/L{ j r-~~-+-~---!...f~..:.....j...::::::....L.::....j......:; ~'J.J-Ii -J f 2.· N ~ () z_{p-'-{-+ i-10~ -.' · s-ob() Additional (Extra) Leak Check Information DGM before Leak Check Vac ("Hg) ---·- -z-1-( lP ll3·'Z..-- Rate lfe/min) DGM After Leak Check ~b'1 1..- 1--{;· I Vac ("Hg) I N ,. Pa~e Lof---l.-Run #_j_ Bo 12.7 5" Port Reference ___,0,__" _ T___ Upstream from next disturbance 30' Downstream from !asl disW.rb:!.n~ Assumed Moisture 4-6% Probe 1.\ ----Cp 0.84 Nozzle ~alibration / ~ '1. -:r--~ ,/ 11-r 2--r-> A vg Dn Z y-<-~ .;ches Gas Bag f-' -i> Console C( Y-Factor \.. {;o C7 / C.Hs l , -t. "'\:')in H,O Barometr\:(.l¥su.res Pbm 1, '? [) in Hg Pb z_"( • z_.'') in Hg P'---,;;:----- Pa • t.8: in H20 Leak Check: pre ft'tmin o-·ObY voc in Hg "2-2- Post , f O·OD'1 tv o·o G-. S.: Water Collected ~ ~ • \ g Time Sampled~ min Review ~ K= K= "' @Tm @Tm Rate (ft3/min) p'V) 7 Field Data Sheet Plant: Enerr. Fuels , Date: fa r~. (f< /, L/ : I , TETCO . . -::;:) E J4 Filter t, coy Sample Box .J,:2../ ·--- Location: Sout~llow Cake Dryer Scrubber Operator: 8 Trav<r.>< Jl Time It Point aP Clock I Min (9) II en'> II c;" H,O) I In DGM Page_l_orl Run# L -- 1 Do N 1 1 12~{t1 1 o ll~GuooojlldJ t·o'-r.o~c2-=r~ll~lz;,ll(3Zlz3z_lc,~l~o! =t-o 2 o 1f '+ ~ q~ ~ ["ZiJ I · o 'L r. o t: 131 ~ t 1 _ z ) 0 _ ¥J ~~1-5 G_ '1 '1-/ Stack Diameter 12. 75" Port Reference --"0'-"--- 1 2 2 2 3 3 3 4 4 4 1 1 1 2 2 2 3 3 3 4 4 4 Total Average '2. 'i?'" {£J I ~-2J ~ IPortsare 7' Upstream from next disturbance C.,-{p 7, 1-"2-• _..-'Ports are 30' Otr.\1fistret~m from li!St disturbance ~~;--r~~~~~~~~~ 7~ Assumed Moisture 4-6% tOO II t17.."1. ~-(~.LV ]II· Ll ITifiKll, I cj, 12.~( 11_ ~2-'S-~ l s--!l~ 1li!s:-5 1 zo ll<1~-~1.2-? II :.z711 i-o:F--1 t·o111"'5li\E\~I01 IJz -51-ll;-3T.75T~~ ?r'f NO II q~-z..--2-.sj II z '{ II [-OI.l-1. i)1/113. II ., (CfT?_u.vr· z 53TZ'o/'lfr 5.~ II ~0 17>-;, t&D II'Tr~Z--<i'lf 11-1:) II~~ -GJ Yll z:r1f-ll~ j'b&o -1 z.s~J-z_5'bf_/P-&-II 1~1 B-1 ~~-b-Jiqt)(?D"'h ll-t-5"'11\·o-+l\-611~1 I() 1-z-~~ z.)C)!z.5H l?Z-11--:t-71-~b- zooii/OCLj.2) -\ 11-i..{> II ~tlt~~ll\l3 lzs--ti'Zk'fl z-v?_l"£.?3 _11 f-01 1-CJ /~-~~ I zzolltot~.t 1-'111 ~~II r-o-t:ITQllf-l.PJITI1-f-z-s~rz."5<tr'Z~1f-& Lfll1-c.rl +Y 'f; -z-Z--1 z {v-II;O) L C) ·Db II·~(, !It-f/ [I -({ 1!2lll f o q I z~L( I Z-3'-{ I Z J~l t s-11 Ct7 G I f;_h zC,OIItD'-I-6-:(r:,IILs--llt·o1-l\·crl~l ll0 lz_-q-o lz.&~J ?~VJ I q-~r~oT-=1:, zfollro5~.'1z-<l!I~J 1-J/+:J Lu'f i~IT\~&~ I ~liS1t~01~11L---I f~. 3 ocll;o ~~ <{"(rt_._L.t:JI r·l) J f·csjiLfll a~[ I z6tf z. 3 vfz..Js--l ~7-11 1-.s-11-CJ 3zoll 1ut5:t-.&Y /II ·7.-q.;IIH\1t·~lll 11\..I I z0:SIZ-3irz3ol ~ez II -:Ji-1 &I ! tt'oll 1 lo \.s-zld-~>II f,\)-1-l r-:-f!ITll~ I -L-vi.!z -si I z 31[ ~ -z_ll1? I :;-~- 3 Wilt I 15" & tiJI 1--s II r. f) 1-1 1. o :}11~1 1 r ~..f lz&5ll3D I Z-3 / I G7'f!IT?T Yo s~o 111-1. q (~_!~~ tli: I L~~ 11-3(~7~~~ II t-~t -;+.~ 'fbC> "c.3-'1 zo ~~[?] tl~l-z 3 7)1-z.-.,[51 . +s ::;. ~ '{ZO 111\.)}. 5'7z-l[. ~~ "JI!-_v 'l:_l t-o ::rll-v-102--rz:q3 r-t351 ,n.>1 >& II 1& I ~ D --No lit t-:f-1. r--;r II ~--~ II, -o z; I t-b" IWll r 11..-IZi 1 I"L~.;-1 7 ~l.9 I c; ~ II 1-1-l yf ...! ~ o lit ( ~ ~ -1 >lf'll~ll c · o"L--·1 ~-C)vll011 \ ~ -t,-11)LS{ I~~~ I~ -5 t, I & z7111i=l-g I 111; 1 t.l ,,q--uIll { ti ~ . .:;---t-Fl 3)t -~i-~q_1~~ ~ .L\~~~ Additional (Extra) Leak Check Information l ') -S"~ \ -o~~ '[,~~~ l\l·<=> DGM before Leak Check Vac ("Hg) Rate (fe/min) DGM After Leak Check )b5-~ 1""~ .-u Vac ("Hg) Probe _z~f!,__ __ Cp 0.84 Nozzle Calibration z 14 7:1~-2"±<;-2-1 ~ Avg Dn 7. f. 'j ~inches Gas Bag (-0 ) Console l{ Y-Factor / -0 () o AH~ f.'--{~ sJn H20 Barometric Pressures Pb 'Z'i-JO -H m m g PbP 2 'f . 2-'J in Hg Po G · -z.. ~.) in H20 Leak Check: Pre-Post J ft'tmin o -oo ~ 0 ·C:.O 1 vacinHg '2.. Z.., ~ Pi rot Rare {) -0 lnH,O 5-S: Water Collected Time Sampled Review Rate (ft3/min) I I O·u ~·5 L-/33-j_ K= K= 'f'}'iJ D ' lA @Tm @Tm g min Yell ow Cake Dryer Baghouse riCIIIJI U l-Jl!) Uii:liU\ Facility Denison Mines Stack Identification North Yellow Cake Dryer Baghouse Date r Barometric Pressure B Pbm in Hg Pbp in Hg N Static Pressure (P0 ) in H20 A Estimated Moisture (Bw,) I % Sample Height from Ground feet Comments: Stack Dia 16 Reference 0 Pons are 57" Upstream from next disturbance Ports arc 468" Downstream from last disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B c D E F 1 4.4 0.70 0.70 2 14.6 2.34 2.34 3 29.6 4.74 4.74 4 70.4 11.26 11 .26 5 85.4 13.66 13.66 6 95.6 15.30 15.30 - Averages: Ts LFiow ---- ll.P -JtJ.P -------- KE'r' => IM~ t3 A. Field Data Sheet Plant: Denison Mines Date ~/t7/l "f. Traverse Time Point Clock Min (B) 1 l'{~tJ> 0 2 lO 3 2o 4 3o 5 LfO 6 so 1 l5~cM c.o 2 '10 3 80 4 'to 5 leO 6 .iO . IC.~<i l't.O DGM (f'l)) --zq_'{,gl,C( ~01 • (.-=J.5'" 309. t:l:JJ "'Jl~-770 )Zl . c.r:r 3 Jo, (~f 3~9. ~1{ "3"t<.. t~u 35'{. !Bo 3£, l· ezo 13c..W.·uo 3:-K..I.l~) ~ Sl. esLf ~p 6.H (;n H,OI (inHaO) Desired Actual •So LJ~ L.~ •"(t-• t('{ .cr'{ .,:so •'-1 ·'~ •1'2.-L • C.{ '·f. ( ·SC t, f,( I. 8t . ,r,. L, '-l f. f. ( .(, ~ \d·o t.{J ·c. a t..{ z.. (,{L ·G.( t.~~ L.:r-;- •C.o •. ,&.~ ,, 3"( ·57' 4 ·Zf> t~ z.~ 1 b0 L ·:!>~ h~ - TETCO Filter (gZo T Sample Box~ Vacuum (inH!I) -'i_ '"{ '{ "( s S_ 'I 'l '{ "{ I( "{ Location: Yellowcake Dryer Baghouse Operator: J(\1. M Q~ o- Temperatures (F) Stack (T,) Probe Probe Out Filter Effluent lO~ l.'-ro 230 l.3o .£5 io1-'2.3o 1..:;H' l,"j{' '4't to~ ?.(.~ Z..lo 2.'10> Sl l41"+-270 'Z.JZ. 'Z.H ... 5«.t '0 '":l-l.~ Z30 !3'0 5'1 lioc,. IZ.·ft 23\ 231 !ir.... 1.07' 170 Z2.( 2-f:f' SB l() .... ZSo Z.C.l-u.t-c.o lo'f l(.Q 2.10 no '0 to8 1SS Lit. Z.1 z. ~~ tc8 Z<(~ Z72. ZT'Z. ~0 lot{ Z•fl· lio Z{O 5":J- Total 9q. o~O l ,r j :z.Z83 / \(.. .!~'U./ \'Z,S ( ./ A ,~ . 71,~v \· '1"t4 \07"·\ Comments: Time Baghou.se ~P Time Baghouse ~P 9 f>tA.trt.\5 ~"' !D"( ct·O ~s~oo g.t, 4'-\'·f\ q.o IS'tU> '\.~ \~:')"! s·r ,s~~ li. \ f"'\ : s ~~ r'it ~ ~<. 5-e ---- DGMI~Il)p (T,.) Out In ,_-[ 1-":1-' 11 1~ .~( 71" 8) 7{ cro ," ~z. '":fr_ S't :~ t:fu 80 1_(._ 8t Cf8 8l' '18 6'{ ere s~ - '1.0 Z,"Z-a/ s '-{, :> Page_\_or_l_ Run# __ i B N ·0 Stack Diameter 16" __ Port Reference _ 0.0"_ Po1'1S are g:___ Upstream from next disturbance Ports are 466'' Downwt:am from last dlStu.rbanc.: Assumed Moisture _....:.....___% Probe "Z.1~l Cp~ Nozzle Calibration . tn •Z.'t~ -Zz.2.. ··u.~ AvgD, • "Z.l2. inches Gas Bag Ambient Air Console ___j Y-Factor I . oot. 6H@ j.fe-;'L inH,O Barometric Pressures Pbm Z. c.{, '3 i) in Hg Pb0 Z '{ · ·t~ in Hg P0 -• '!,&.{ in H20 Leak Check: Pre ft'lmin 0 :-;o:(' ,•..:lnHll '2.0·~ ~ 0.0<'3 ~ Pitm,ii= Q•O e>O lnHP ,.~ 1.0 Water Collected G:, ·l g Time Sampled ____1_10 min Review ~ K= K @Tm rn:.-T -.. Grizzly Baghouse Prelim 12 pts blank Facility Denison Mines Stack Identification Grizzlv Baghouse Date i,( ·~ ft't r Barometric Pressure Pbm ~'(. ~0 in Hg Pbr 'lc.4., z~ in Hg N 'AOB Static Pressure (PG) _ .l'l{'C., in 1-1,0 Estimated Moisture (Bw,) I ~-0 Sample Height from Ground 'lo feet Comments: Slack Dia , 18.75 Rcli:rcnce: 3.0 Must use 36" probe or longer to keep bo:-: outside handrail P<lilS are 24.5" UpstreJm from ne.\t disturbance Ports ar~ 48" Dm111strearn from last disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B c D E F I 2.1 0.50 3.50 ' CJ (,O 1o 2 6.7 1.26 4.26 3 I 1.8 2.21 5.21 .o)~ l/ 4 17.7 3.32 6.32 5 25.0 4.69 7.69 6 35.6 6.68 9.68 •&1'-f , .. 7 64.4 12.08 15.08 8 75.0 14.06 17.06 9 82.3 15.43 18.43 ''"6 11( 10 88.2 16.54 19.54 II 93.2' 17.48 20.48 ,,,., ""'1 12 97.9 18.25 21.25 Averages: Ts L Flow ---- t.P v'~P -------- L Flow! ."lP . KEY=> IV"~ Field Data Sheet riiter~TETCO ~ lt{) Sample Go,,__£_ Pnge _\__or_l_ Run #_f_ Plant: Denison Mines Dute: V ( \ "!{ 1 '"( Location: Grizzly Baghouse Operator: l't\ . M ~AAt!l\ltoJtt- 6 Travers~ Time DGM L;J 6H !w-.H;Ol Vacuum T;!mperaturcs ('F; DGM TernD (f.) PO!tJi Clock Min (e) Ill'! Desired Actual (nof/,:) StadqT.) Probe Ph:::bcOul Filter Effiuent Out In . 1 -~·.t~ 0 ~Sol Cl•l .n .,,., L<1-L<:~ ~ 70 7.:FJ 1.."70 27'0 5_"'\ -:t'f (,~ ... I AO B N 2 lo 'ioo-110 ·•":1-o ''· .,0 u~o 3 12. ,,I.. I) z t-) 2C. ,)' 5( 9~ ":f-2-~lad. Diamerc:r I~. 75" Pon Reference ~ 3 40 'lll. 4C.o ·CG.S ~.. S<.( L. SL{ 3 ;{' zc,, 'Z-38 '2.38 Sl 93 "1--1-Por\s are 24.5" Upstr~am from next disturbance 4 (,o r.t~S.o1) • 6"1'1. 1·111 i·'f.. L{ 1"1 l.So 1.40 Zo.fO 57. t:{) So Por~are 48• • Downme3m from last disturbance 5 So 't{3. ''30 • o4'-\.~o '·So 'i IB l7() 'Z.'-{1 t."f't S'Z. <-i.3 St Assumed ~~1visture 1 %, 6 IOO "'( '\oo .l ,.0 •o'l~ 1. <iZ. "2-·e.l.. 'I IS 270 2,{{ 2(? 52. Ci"! f?2 Probe 3~ -l7 Cp 0.84 7 JZO 'f 8~LS?c: • •'lO I ·'t I Lctl 'i ,q 210 Z'3o l~ 54 '\3 -~~ 8 l~o 5 Dl. .300 ·1170 t ·•U "~ l I.( -RQ 2'i& '2. L(o 'Z.,'to s~ '13 B~ L Nozzk Calibr:.tion .'-(o'{ ·'to'\ _:j-aC(. .'-lo0 9 11#0 52. 'i. 13;' -o~8 l-S{ '· sr 4 an zso z<oo Z"O 55 'io 83 A•!; Do • "\v ll{ inches J 10 ,go s 41 . itt:~i> ... <.., 1. R8 l.i~ '{ 19 lf.C z. 70 Z"'TO C.o 8+ ec Gas Bag Ambient Air 11 too 551.. II{ •07( l.. oc.{ z.oo.l t{ So 't '" l. "~ u .. ~ '{'{ 8't g, Console __ ,._ __ 12 2.20 5'1~·,l0 .elo l·''tl I.Cf I '{ 'af 7r.f '-z. C.(<; 'l Y'l 4{l s' ~'2.. Y-Factor I.OO 1.. 1 •1:zt 'Z.'lo S'~ 4 . (. "'l-'2. .o~1 t. St t·8Z.. 4 ~0 1. £,~ tq'\ l'i.3 ,, 83 6( 2 zc.o Ltl.€6~ ·01Z. l· 'lC.! J.C\(, '1 Bt 2(,l z'iq 2-'fli. ~~ Jl{ Bo ~"( t>H@ \..(e{2)nH20 Barorn~tric Prc:ssures 3 290 (.2.'l,,11 . .,;'-(_ t.ct.. Z-o'-t.{ -~1.t z~ 'Z'fU Zf'i S\ i't et Pbm z..q, ~ in Hg 4 3oO (.,.•,P.Cflf' .e8'z. z.t~ 2.z3 " g~ 't,(,Z. z-r) z.;, 5<i ea fl'Z.. 5 4 II J 3oO IJ f_'4,.Cflf' ll .eB?..II 1·t'!>I 2.Z"\II 'i II gt.{ I 't,(,Z.I Z-{)1 2l',15<i II ee I B'Z.. Pbr "Z.Y.•z:r inHg 5 6 ~ 7 8 9 , 10 11 12 ~ Total Av~r:~ge. Comments 31.0 G.fo (.o"f-f ·¥1~ '2-\'j' ~40 t-es. '&Jo .o'1) l.o~ 3"o '1o'i. O"li> • 0"'( l·1c.( 38o 71-'0 ·B'S-( •oSlo-t.{{ ~oo ,3&>.79o ··~~ ,.-( ( 4ZD '15"2 .ql-{ ·•){ l·fo 'l{tfo it..R~:( •0~3 ._,o{l.o{ LfC,, 1B'f · 'i~o ·<>55 •·10 \f.: t.l Y Qu eco .1.qr / 4l~ .2 tt+--" ,; ~. z.B~ ~s~ ft s~~ J8&.{.o5o v • 2,{<'f>/ 'l-lf y 't ·ocf ~ , .. ., cf 4 '-~ -1{ It ,,.{f '-j l.(O Lf v~"{ ~ lrfO l{ '{ "l.octo l-~3~ / RCf z 'fo 90 z.z.{ ~z.. 130 9'2.. z.'{'{ .,_,. 7_ l1o '\'2.-Z.!>~ set -t.C.~ 8'f isa ttf Qt.{/ 82..1- 1.'t~ tc.t$ .H~ [')'[ Z31 C:T Zl.Cf zz.q ({3 2 "t'{ 'L'I'f. {.l(, z. 1" 2.. l~Z. (f~ 2.{:5 .2..1:) .57_ 'Z.-D"B z76 s~ 'Z'10 Z7o '0 8B_ i6z. Pc; --c)(, inH.,O m, e'l,., Leak Check Pre Post ~b ~2. ft 'im:nO• &:IO{q tafo '8-:., voconllg_l_~ ~.Q ~B g'{ Sct gt{ P1:vtR:ue .'20 .1. v (;H B_L lnH,O ~ ~ 'f't 9~ Water CoJiected 12 • 't g Time Sampled '180 mm 4,013 Rcvtew ~ <a£4·~ K~ @T"' K= @Tm South Yellow Cake Scrubber Sample Recovery Gas Analysis Data (ORSAT) Yellow Cake Dryer Baghouse Sample Recovery Gas Analysis Data (Ambient) Grizzly Baghouse Sample Recovery Gas Analysis Data (Ambient) Chain of Custodies Lab Analysis APPENDIXC c South Yell ow Cake Dryer Scrubber lVlt 1 t1VU ) Facility: Em:rt>.v Fuels Stack Identification: SYC Scrubber ~~~~~-------------------------- IMPINGERS Run: \ Sample Box: E. Impinge•· Number 2 I 3 1 4 1 5 6 Initial Volume Df hquid (H,O) in impmgC , (ml) 100 I drc pout I 100 I '>1lica <fd --< ~ Final (g) Initial (g) Net (g) Total (g) y::,~, I j<:, TM£1NGERS Run: 2 Sample Box: E. {,20~ lmpmgcr Num6er 2 I 3 I 4 I ~ 6 hllti:ll Volume of liqltitl (HzO) in impingers, (m[) dt·o~ out 10 I dr p ClUI I 100 I Silic:1 Gd I Initial (g) Net (g) Total (g) L-( 3 7 .cz !MI!U'sGERS Run: Sample Box: lmpinger Number 2 I 3 I 4 I s G Initial Volume of liquid (H20) in ill1t>ingcrs; (ml) drop out 100 I dro p out I 100 I Sili"a Gd " Final (g.) Initial (g) Net (g) Total (g) IMfi~GERS Run: Sample Box: lmpinger ~um6cr 1 2 I 3 I 4 I 5 6 .. Final (gl Initial (g) Net (g) Total (g) ~ Plant &, ~/ tTr fi, ~ U Analytical Method 7 0RSA T Date &I~)~/ Gas Test No. I ;: -(.),5 .... Gas Bag No . Ambient Temp . F* Operator Date & It<; IlL/ Gas Test No. "'2--- Gas Bag No. E--os- Ambient Temp ~ Operator Date Gas Test No. ____ _ Gas Bag No. ____ _ Ambient Temp _____ _ Operator ------ Location. ___ 7-r--'t-/-'C;;;..._ ___________ _ lr----,----~~---~---~l~---~---~l Average Aetual Ruding Actual Net Net Aclunl Actual Net Net Net Actual Reading Actual Reading Actual Reading Net Nrt (. (: I ~·l- Net Net Volume I Js-- Average Net Volume (. c ( &- Average Net Volume CO is not measured, as it has the same molecular weight as N2 Yell ow Cake Dryer Baghouse "t1ITZZLy ,.,.,.. ' Facility: 1-nt:l~t;v Fuels Date:_~__._/ 1-'-7 .:......:{/_Lj_,___ Stack Identification: leJ \o t0 (..:a. \.<..e... :Du ~Ia ov ~--( IMPJNGERS Run: l Sample Box: D Filter Number lmpinger Number (j 1_.o;f' 2 I 3 I 4 I s 6 IMPJ~GEB~ Filter Number IMJ!II:':IGER~ Fi Iter Number Final (g) Initial (g) Net (g) Final (g) Initial (g) Net (g) Final (g) Initial (g) Net (g) 100 I I C,O'i.o {p(~-1 -I(.L3 Run: 110 Run: iOO Initial Volume ofllquicl {1-110) in imping.~rs. (ml) 100 I . I !i•Ji,:u ( •<'~ I I I 1 ' • ' . (..( b I l ~1~·3 9tO,~ utll-1 (,J }·' 71<61. 7f -·3 . (._ l 0·.5 Total (g) Co • { Sample Box: [mpmger Number 2 I 3 I 4 I 5 6 Silica Gel Total (g) Sample Box: Impinger Number 2 I 3 I 4 I 5 6 Silica Gd Total (g) Grizzly Baghouse Method 5 Facility: Energy Fuels Date: __ ~ ....... (J...:r 8 .... 1~/....:Y __ Stack Identification: ..:G::..:r.=izz=l~y _______________ _ IMPINGERS Filter Number IMPINGERS Filter Number IMPINGERS Filter Number Final (g) Initial (g) Net (g) Run: 100 I t>-ss.o (po '-l · 0 -c.!'i-0 Sample Box: 2 lmpinger Number I 3 I 4 I s Initial Volume ofnc1uiil (A~O) in impingcrs, {ml) I 00 I I Silica Gel I ' • • ~ 1..31 J «...( (p( fj I -:r-q51 . .s C.l(,,\ "l ~. 3 910·3 IS-3 5'.~ 1.( l· z.. _______ Total (g)==:===:::I'Z.=· =9==- Run: Sample Box: Lmpinge•· Number 1 2 3 I 4 I s Initial Volume of liquid (H10) in implngcr.;, (rill) 100 100 I I Silica Gel I D 6 . 6 Final (g) ----f--------4-----4-----+----1----- Initial (g) ___ -lf--------4-----4-----+----1----- Net (g)====:!'======'====:!===='====::::!:==== Total (g) Run: Sample Box: 1 2 lmpinger Number I 3 I 4 I 5 6 Initial Volume of liquid (H20) in lmping~:rs, (ml) 100 100 I I 'ilic;J Oct I Final (g) ----11------l-----f~-----+----+---­ lnitial (g) ----11------1-----f-----+----+---- Net (g)===:=!:===::::!::::===!:::·===='=====:!==== Total (g)======== Temperature on Receipt __ _ Test America Custody Record ·. Drinking Water? Yes 0 ·No 0 THE LEADER IN ENVIRONMENTAL TESTING T~-4124 (1007) Glism --pr(J/iJr;t.Mans.oiJr _ D?t~. Chsln of Cusrodv Number Tetco Deao Kit.!=hen \6/19/2014 .. Addre$$1 T~ Nfm:112~(Ates ~]If~ Numbpr _ ~bfl/umlifN' I 1 · · 391 East 620 South 801-492-9106 Page of City I State !ZiD Code Site Contact Lab Contact Analysis (Attach list if American Fork Ut 84003 Stott Christensen, Garren Palmer more space is needed) . P.CJii85<t Namfl:M:d L<lW!lioo lStatsl c;.msrM'sy6ill Nunlber Energy Fuels 2014 2nd Quarter ,, Special Instructions! CQ(Jirai;tlP·Jt'r:JIItse Ottfor/Dubco No. Containers & 1 0 Conditions of Receipt Matrix PreseNatives 0 "' .... ~ "" N N "' ":' N -b Sample 1.0. No. and Description I ~ ~ @ 8 ei ~5 z :r .. "' ::) .. Date Time ~ "ti 'a ! ~ H a: .... (Containers for each sample may be combined on one line) _, ~ ~ ~ ~ ~ ~:1! I ... « II) 6/17/~ R1 Dryer BH filter (6207) and beaker 10:00 -. ' '1 X Klx X X -,-8:00 lx· R1 SYC Scrubber filter (6206) and beaker 6/16,17/14 X X! X X R2 SYC Scrubber filter (6208) and beaker 6/17;18/14 i ,I 13:00 ;I X X )( I X. X r R1 Grizzly filter (6210) and beaker 6/18/14 8:00 X X X -r --I I . r--I I I I I ' ; Pcssible Hazatd li;/QfllirtaBtl::m I St~mple D<'SpG$jll (A fee may be assessed if samples are retained 0 Non-Hazard 0 Flammable 0 Skin Irritant 0 PoisonS 0 Unknown 0 Retum TD Client 0 Disposal By Lab 0 Archive For ___ Months Ienger than 1 month) ----------~ Rilquliilments (SpedljJ. 0 7 Days 0 14 Days 0 21 Days 1.R~d8y Time 2.R~ed8y :I; ReJinquiShiid 8y 3. ReceiVed flU' I ~me ComtrdJn:r;- When Complete Email to: Dean or Paul, tetco@ tetco·l,lt.com DISTRIB!Jr/ON: I'YP.fTC • RelutT>ed k> Cilent wilh Repotl[ CAili'AI'fY • Sl!lys t>~frh the SStTip/e; Pllm • AeitiC::OI>'I ·'""'· SDGNo. Order No. 48381 TestAmerlca Inc rptSTLRchTitle v3.73 Analytical Data Package Prepared For Denison Mines (USA) Corp. Radiochemical Analysis By TestAmerica Inc 2800 G. W. Way, Richland Wa, 99354, (509)-375-3131. Assigned Laboratory Code: Data Package Contains 16 Pages Report No.: 61895 Results in this report relate only to the sample(s) analyzed. Client Sample ID (List Order) Lot-Sa No. Work Order Report DB ID R1 Dryer BH J4F240448-1 M36EH1AE 9M36EH10 filter(6207)and be R1 Dryer BH J4F240448-1 M36EH1AA 9M36EH10 filter(6207)and be R1 Dryer BH J4F240448-1 M36EH1AC 9M36EH10 filter(6207)and be R1 Grizzly filter(6210)and J4F240448-4 M36EL1AC 9M36EL10 be a R1 Grizzly filter(6210)and J4F240448-4 M36EL1AA 9M36EL10 be a R1 SYC Scrubber J4F240448-2 M36EJ1AE 9M36EJ10 filter(6206)an R1 SYC Scrubber J4F240448-2 M36EJ1AA 9M36EJ10 filter(6206)an R1 SYC Scrubber J4F240448-2 M36EJ1AC 9M36EJ10 filter(6206)an R2 SYC Scrubber J4F240448-3 M36EK2AE 9M36EK20 filter(6208)an R2 SYC Scrubber J4F240448-3 M36EK1AA 9M36EK10 filter(6208)an R2 SYC Scrubber J4F240448-3 M36EK1AC 9M36EK10 filter(6208)an Batch No. 4176035 4176037 4176039 4176035 4176037 4176035 4176037 4176039 4176035 4176037 4176039 1 of 16 Test America THE LEADER IN ENVIRONMENTAL TESTING Certificate of Analysis August 22, 2014 Denison Mines (USA) Corp I 050 17th Street, Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab Project Name Sample Type SDGNumber I. Introduction June 24, 2014 Energy Fuels 2014 2nd Quarter Four (4) Stack Filter Samples 48381 CASE NARRATIVE On June 24, 2014, four stack filter samples were received at TestAmerica's Richland laboratory for radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification numbers as described on the cover page of the Analytical Data Package report form. The samples were assigned to Lot Numbers J4F240448. II. Sample Receipt The samples were received in good condition and no anomalies were noted during check-in. III. Analytical Results/Methodology The analytical results for this report are presented by laboratory sample ID. Each set of data includes sample identification information; analytical results and the appropriate associated statistical uncertainties. The analysis requested was: Alpha Spectroscopy Thorium-228, -230, -232 by method RL-ALP-001 Uranium-234, -235, -238 by method RL-ALP-004 Gas Proportional Counting Pb-210 by method RL-GPC-011 Alpha Scintillation Radium-226 by method RL-RA-001 2 of 16 Denison Mines (USA) Corp August 22, 2014 IV. Quality Control The analytical result for each analysis performed includes a minimum of one laboratory control sample (LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments" section. V. Comments Alpha Spectroscopy Thorium-228, 230, 232 The batch blank result for Th-230 was above the achieved MDA; a recount confirmed results and there is no sample remaining for reanalysis. The achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to historical process knowledge. There is no sample volume remaining for re-analysis. Data is reported. Except as noted, the LCS, batch blank and sample results are within acceptance limits. Uranium-234, 235, 238 Sample R2 SYC Scrubber had smeared spectra in the original count of this batch. The sample was stripped and rerun through cartridges. Upon completion of reanalysis, tracer yield recovered low at 12%. This sample fails and data is reported for client review. Initial count for blank had a result for U-238 and U-234 that exceeds MDA. This sample was stripped and reprocessed, with acceptable results. The achieved MDA of samples exceed CRDL. Except as noted, the LCS, batch blank and sample results are within acceptance limits. Gas Proportional Counting Pb-210 Tracer yield for batch 4176038 were insufficient for completion of the required analysis. No remaining sample for reanalysis. No data reported. Alpha Scintillation Radium-226 The CRDL was not met for the samples or QC for batch 4176039 due to method limitations for the matrix. The tracer yields and LCS recovery meet acceptance criteria. The blank activity is below the MDA and sample results show no indication of method contribution. Except as noted, the LCS, batch blank and sample results are within acceptance limits. I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically and for completeness, for other than the conditions detailed above. The Laboratory Manager or a designee, as verified by the following signature has authorized release of the data contained in this hard copy data package. Reviewed and approved: ~Ma~ Robin Ebe1- Project Manager 3 of 16 Drinking Water Method Cross References DRINKING WATER ASTM METHOD CROSS REFERENCES Referenced Method lsotope(s) TestAmerica Richland's SOP N o. EPA 901 .1 Cs-134, 1-131 RL-GAM-001 EPA 900.0 Alpha & Beta RL-GPC-001 EPA 00-02 Gross Alpha (Copreclpitation) RL-GPC-002 EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002 EPA 903.1 Ra-226 RL-RA-001 EPA 904.0 Ra-228 RL-RA-001 EPA 905.0 Sr-89/90 RL-GPC-003 ASTM D5174 Uranium RL-KPA-003 EPA 906 .0 Tritium RL-LSC-005 -1 Results in this report relate only to the sample(s) analyzed. Uncertainty Estimation TestAmerica Richland has adopted the internationally accepted approach to estimating uncertainties described in "NIST Technical Note 1297, 1994 Edition". The approach, "Law of Propagation of Errors", involves the identification of all variables in an analytical method which are used to derive a result. These variables are related to the analytical result (R) by some functional relationship, R = constants * f(x,y,z, ... ). The components (x,y,z) are evaluated to determine their contribution to the overall method uncertainty. The individual component uncertainties (ui) are then combined using a statistical model that provides the most probable overall uncertainty value. All component uncertainties are categorized as type A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the components, such as sample homogeneity, are combined with the component uncertainty as the square root of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result is the combined uncertainty (uc) multiplied by the coverage factor (1,2, or 3). When three or more sample replicates are used to derive the analytical result, the type A uncertainty is the standard deviation of the mean value (S/?n), where Sis the standard deviation of the derived results. The type B uncertainties are all other random or non-random components that are not included in the standard deviation. The derivation of the general "Law ofPropagation of Errors" equations and specific example are available on request. TestAmerica Inc rptGenerallofo vJ. 72 I l 4 of 16 Action Lev Batch Bias COCNo Count Error (#s) Total Uncert (#s) Uc-Combined Uncertainty. (#s), Coverage Factor CRDL (RL) Lc Lot-Sample No MDCI MDA Primary Detector Ratio U-234/U-238 Rst/MDC RstffotUcert Report DB No RER SDG Sum Rpt Alpha Spec Rst(s) Work Order Yield TestAmerica Inc rptGenerallnfo v3. 72 Report Definitions An agreed upon aetivity level used to trigger some action when the final result is greater than or equal to the Action Level. Often the Action Level is related to the Decision Limit. The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed together. Defined by the equation (Result/Expected)-! as defined by ANSI Nl3.30. Chain of Custody Number assigned by the Client or TestAmerica. Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background. All known uncertainties associated with the preparation and analysis of the sample are propagated to give a measure of the uncertainty associated with the result, Uc the combined uncertainty. The uncertainty is absolute and in the same units as the result. The coverage factor defines the width ofthe confidence interval, I, 2 or 3 standard deviations. Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmerica "default" nominal detection limit. Often referred to the reporting level (RL) Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume associated with the sample. The Type I error probability is approximately 5%. Lc=(l.645 * Sqrt(2*(BkgmdCnt!BkgmdCntMin)/SCntMin)) * (ConvFct/(Eff*Yld*Abn*Vol) * IngrFct). For LSC methods the batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count is zero. The number assigned by the LIMS software to track samples received on the same day for a given client. The sample number is a sequential number assigned to each sample in the Lot. Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume with a Type I and II error probability of approximately 5%. MDC= ( 4.65 * Sqrt((BkgmdCnt/BkgmdCntMin)/SCntMin) + 2.7l/SCntMin) * (ConvFct/(Eff * Yld * Abn *Vol)* lngrFct). For LSC methods the batch blank is used as a measure of the background variability. The instrument identifier associated with the analysis of the sample aliquot. The U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural uranium in NIST SRM 4321C is 1.038. Ratio of the Result to the MDC. A value greater than 1 may indicate activity above background at a high level of confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of2 a value greater than 1 may indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers associated with the result. Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order Number. The equation Replicate Error Ratio= (S-D)/[sqrt(TPUs2 + TPUd2)] as defined by ICPT BOA where S is the original sample result, Dis the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the total uncertainty ofthe duplicate sample. Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt. The sum of the reported alpha spec results for tests derived from the same sample excluding duplicate result where the results are in the same units. The LIMS software assign test specific identifier. The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method. 5 of 16 Sample Results Summary Date: 22-Aug-14 TestAmerica Inc Ordered by Method, Batch No., Client Sample ID. Report No. : 61895 SDG No: 48381 Client ld Tracer Batch Work Order Parameter Result+-Uncertainty ( 2s) Qual Units Yield MDL CRDL RER2 4176037 RICHRC5011 R1 Dryer BH filter(6207)and be M36EH1AA Th-228 3.74E-09 +-1.5E-08 u uCi/Sample 41% 3.47E-08 3.00E-15 Th-230 5.55E-07 +-1.3E-07 uCi/Sample 41% 9.77E-09 3.00E-15 Th-232 4.33E-09 +-1.1E-08 u uCi/Sample 41% 2.48E-08 3.00E-15 R1 Grizzly filter(621 O)and bea M36EL1AA Th-228 1.03E-07 +-4.5E-08 uCi/Sample 35% 4.34E-08 3.00E-15 Th-230 1.87E-05 +-3.0E-06 uCi/Sample 35% 2.89E-08 3.00E-15 Th-232 2.38E-07 +-6.9E-08 uCi/Sample 35% 2.63E-08 3.00E-15 R1 SYC Scrubber filter(6206)an M36EJ1AA Th-228 2.08E-08 +-2.4E-08 u uCi/Sample 24% 3.27E-08 3.00E-15 Th-230 1.47E-07 +-6.5E-08 uCi/Sample 24% 4.79E-08 3.00E-15 Th-232 5.57E-09 +-1.2E-08 u uCi/Sample 24% 1.51 E-08 3.00E-15 R2 SYC Scrubber filter(6208)an M36EK1AA Th-228 2.69E-09 +-1.1 E-08 u uCi/Sample 41% 2.63E-08 3.00E-15 Th-230 2.25E-07 +-6.2E-08 uCi/Sample 41% 2.79E-08 3.00E-15 Th-232 2.14E-08 +-1.8E-08 uCi/Sample 41% 1.84E-08 3.00E-15 4176035 FFSR R1 Dryer BH filter(6207)and be M36EH1AE U-234 7.08E-04 +-1.6E-04 uCi/Sample 99% 3.10E-05 9.00E-15 U-235 1.48E-05 +-1.8E-05 u uCi/Sample 99% 2.39E-05 9.00E-15 U-238 9.70E-04 +-2.1E-04 uCi/Sample 99% 2.61E-05 9.00E-15 R1 Grizzly filter(6210)and bea M36EL1AC U-234 2.45E-05 +-3.0E-05 u uCi/Sample 77% 4.70E-05 9.00E-15 U-235 1.40E-05 +-2.1 E-05 u uCi/Sample 77% 2.94E-05 9.00E-15 U-238 4.65E-05 +-4.0E-05 u uCi/Sample 77% 4.70E-05 9.00E-15 R1 SYC Scrubber filter(6206)an M36EJ1AE U-234 6.75E-03 +-1.1 E-03 uCi/Sample 84% 1.24E-04 9.00E-15 U-235 2.67E-04 +-9.6E-05 uCi/Sample 84% 6.19E-05 9.00E-15 U-238 6.94E-03 +-1.2E-03 uCi/Sample 84% 1.18E-04 9.00E-15 R2 SYC Scrubber filter(6208)an M36EK2AE U-234 7.92E-06 +-2.4E-06 uCi/Sample 12% 3.28E-07 9.00E-15 U-235 5.02E-07 +-3.5E-07 uCi/Sample 12% 2.33E-07 9.00E-15 U-238 8.35E-06 +-2.5E-06 uCi/Sample 12% 2.54E-07 9.00E-15 4176039 RL-RA-001 R1 Dryer BH filter(6207)and be M36EH1AC Ra-226 4.21 E-07 +-1.1 E-07 uCi/sample 100% 7.19E-08 9.00E-14 R1 SYC Scrubber filter(6206)an M36EJ1AC Ra-226 2.65E-07 +-9.6E-08 uCi/sample 66% 1.02E-07 9.00E-14 TestAmerlca Inc RER2 -Replicate Error Ratio= (S-D)/[sqrt(sq(TPUs)+sq(TPUd))) as defined by ICPT BOA. rptTALRchSaSum U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less tban tbe Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or mary2 V5.3.3 not identified by gamma scan software. A2002 6 of 16 Report No. : 61895 Client ld Batch Work Order Parameter 4176039 RL-RA-001 R2 SYC Scrubber filter(6208)an M36EK1AC Ra-226 No. of Results: 27 Sample Results Summary TestAmerica Inc Ordered by Method, Batch No., Client Sample 10. Date: 22-Aug-14 SDG No: 48381 Result+-Uncertainty ( 2s) Qual Units Tracer Yield 2.64E-07 +-9.5E-08 uCi/sample 91% MDL CRDL RER2 7.93E-08 9.00E-14 TestAmerica Inc RER2 -Replicate Error Ratio= (S-D)/[sqrt(sq(TPUs)+sq(TPUd))) as defined by ICPT BOA. rptTALRchSaSum mary2 V5.3.3 A2002 7 of 16 QC Results Summary Date: 22-Aug-14 TestAmerica Inc Ordered by Method, Batch No, QC Type,. Report No. : 61895 SDG No.: 48381 Batch Tracer LCS Work Order Parameter Result+-Uncertainty ( 2s) Qual Units Yield Recovery Bias MDL RICHRC5011 4176037 BLANK QC, M36K11AA Th-228 1.02E-10 +-1.3E-10 u uCi/Sample 31% 2.10E-10 M36K12AA Th-228 -2.87E-11 +-7.7E-11 u uCi/Sample 26% 2.66E-10 M36K11AA Th-230 7.53E-10 +-3.1E-10 uCi/Sample 31% 7.04E-11 Th-232 4.16E-11 +-7.7E-11 u uCi/Sample 31% 1.47E-10 4176037 LCS, M36K11AC Th-230 1.11E-08 +-1.7E-09 uCi/Sample 79% 98% 0,0 2.19E-11 FFSR 4176035 BLANK QC, M36KT2AA U-234 2.05E-08 +-9.0E-08 u uCi/Sample 45% 2.23E-07 U-235 3.26E-08 +-5.4E-08 u uCi/Sample 45% 1.11 E-07 U-238 9.14E-08 +-1.0E-07 u uCi/Sample 45% 1.98E-07 4176035 LCS, M36KT1AC U-234 7.54E-07 +-2.1E-07 uCi/Sample 81% 77% -0.2 2.84E-08 U-238 9.78E-07 +-2.6E-07 uCi/Sample 81% 95% -0.1 3.99E-08 RL-RA-001 4176039 BLANK QC, M36K41AA Ra-226 2.99E-10 +-2.3E-10 u uCi/sample 93% 3.41E-10 4176039 LCS, M36K41AC Ra-226 4.15E-08 +-8.5E-09 uCi/sample 100% 83% -0.2 4.04E-10 No. of Results: 12 TestAmerica Inc Bias -(Result/Expected)-I as defined by ANSI N13.30. rptSTLRchQcSum U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or mary V5.3.3 A2002 not identified by gamma scan software. a of 16 FORM I Date: 22-Aug-14 SAMPLE RESULTS Lab Name: T estAmerica Inc SDG: 48381 Collection Date: 6/17/201410:00:00 AM Lot-Sample No.: J4F240448-1 Report No.: 61895 Received Date: 6/24/2014 10:40:00 AM Client Sample ID: R1 Dryer BH filter(6207)and be COC No.: Matrix: SOLID Ordered b~ Client Sample I D. Batch No. Result Count Total MDL, Rpt Unit, Yield Rst/MDL, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert(2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Prep Date Size Size Detector Batch: 4176035 FFSR Work Order: M36EH1AE Report DB ID: 9M36EH10 U-234 7.08E-04 1.2E-04 1.6E-04 3.1 OE-05 uCi/Sample 99% (22.8) 7/15/14 10:04 p 1.0 0.00116 ALP1 8.28E-06 9.00E-15 (8.7) Sample Sample U-235 1.48E-05 u 1.8E-05 1.8E-05 2.39E-05 uCi/Sample 99% 0.62 7/15/14 10:04 p 1.0 0.00116 ALP1 5.81E-06 9.00E-15 (1.6) Sample Sample U-238 9.70E-04 1.4E-04 2.1 E-04 2.61 E-05 uCi/Sample 99% (37.2) 7/15/14 10:04 p 1.0 0.00116 ALP1 6.55E-06 9.00E-15 (9.4) Sample Sample Ratio U-2341238 = 0.7 Batch: 4176037 RICHRC5011 Work Order: M36EH1AA Report DB ID: 9M36EH1 0 Th-228 3.74E-09 u 1.5E-08 1.5E-08 3.47E-08 uCi/Sample 41% 0.11 7/24/14 03:49 a 1.0 0.98985 ALP126 1.33E-08 3.00E-15 0.51 Sample Sample Th-230 5.55E-07 9.0E-08 1.3E-07 9.77E-09 uCi/Sample 41% (56.8) 7/24/14 03:49 a 1.0 0.98985 ALP126 5.36E-09 3.00E-15 (8.9) Sample Sample Th-232 4.33E-09 u 1.1 E-08 1.1 E-08 2.48E-08 uCi/Sample 41% 0.17 7/24/14 03:49 a 1.0 0.98985 ALP126 9.43E-09 3.00E-15 0.79 Sample Sample -- Batch: 4176039 RL-RA-001 Work Order: M36EH1AC Report DB ID: 9M36EH10 Ra-226 4.21E-07 6.5E-08 1.1 E-07 7 .19E-08 uCi/sample 100% (5.9) 8/21/14 08:17 p 1.0 0.9898 ASC1MB 3.40E-08 9.00E-14 (7.9) g g No. of Results: 7 Comments: TestAmerica Inc MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.3.3 A2002 9 of 16 FORM I Date: 22-Aug-14 SAMPLE RESULTS Lab Name: TestAmerica Inc SDG: 48381 Collection Date: 6/18/2014 8:00:00 AM Lot-Sample No.: J4F240448-4 Report No.: 61895 Received Date: 6/24/2014 10:40:00 AM Client Sample ID: R1 Grizzly filter(6210)and bea COC No.: Matrix: SOLID Ordered b~ Client SamEie 10, Batch No. Result Count Total MDL, Rpt Unit, Yield RstJMDL, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert(2 s) Action Lev Lc CRDL(RL) RstJTotUcert Prep Date Size Size Detector Batch: 4176035 FFSR Work Order: M36EL 1AC Report DB ID: 9M36EL 10 U-234 2.45E-05 u 2.9E-05 3.0E-05 4.70E-05 uCi/Sample 77% 0.52 7/15/14 10:06 p 1.0 0.00102 ALPS 1.29E-05 9.00E-1S (1 .6) Sample Sample U-235 1.40E-05 u 2.1E-OS 2.1 E-OS 2.94E-OS uCi/Sample 77% 0.48 7/15/1410:06 p 1.0 0.00102 ALPS 6.83E-06 9.00E-1S (1 .3) Sample Sample U-238 4.65E-05 u 3.9E-OS 4.0E-OS 4.70E-OS uCi/Sample 77% 0.99 7/1S/14 10:06 p 1.0 0.00102 ALPS 1.29E-OS 9.00E-15 (2.3) Sample Sample Ratio U-2341238 = 0.5 Batch: 4176037 RICHRC5011 Work Order: M36EL 1AA Report DB ID: 9M36EL 10 Th-228 1.03E-07 4.2E-08 4.SE-08 4.34E-08 uCi/Sample 3S% (2.4) 7/24/14 03:SO a 1.0 0.98825 ALP129 1.70E-08 3.00E-1S (4.6) Sample Sample Th-230 1.87E-05 S.OE-07 3.0E-06 2.89E-08 uCi/Sample 35% (646.5) 7/24/14 03:SO a 1.0 0.98825 ALP129 1.11E-08 3.00E-1S (12.3) Sample Sample Th-232 2.38E-07 5.7E-08 6.9E-08 2.63E-08 uCi/Sample 3S% (9.1) 7/24/14 03:50 a 1.0 0.98825 ALP129 1.00E-08 3.00E-1S (6.9) Sample Sample -~ --~ ·--- No. of Results: 6 Comments: TestAmerica Inc MDCjMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.3.3 A2002 10 of 16 FORM I Date: 22-Aug-14 SAMPLE RESULTS Lab Name: TestAmerica Inc SDG: 48381 Collection Date: 6/16/2014 8:00:00 AM Lot-Sample No.: J4F240448-2 Report No.: 61895 Received Date: 6/24/2014 10:40:00 AM Client Sample ID: R1 SYC Scrubber filter(6206)an COC No.: Matrix: SOLID Ordered b~ Client Sample 10, Batch No. Result Count Total MDL, Rpt Unit, Yield Rst/MDL, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Prep Date Size Size Detector Batch: 4176035 FFSR Work Order: M36EJ1AE Report DB ID: 9M36EJ10 U-234 6.75E-03 4.3E-04 1.1E-03 1.24E-04 uCi/Sample 84% (54.4) 7/15/1410:05 p 1.0 0.00105 ALP3 4.14E-05 9.00E-15 (11.8) Sample Sample U-235 2.67E-04 8.7E-05 9.6E-05 6.19E-05 uCi/Sample 84% (4.3) 7/15/14 10:05 p 1.0 0.00105 ALP3 1.87E-05 9.00E-15 (5.5) Sample Sample U-238 6.94E-03 4.3E-04 1.2E-03 1.18E-04 uCi/Sample 84% (58.9) 7/15/14 10:05 p 1.0 0.00105 ALP3 3.91E-05 9.00E-15 (11 .9) Sample Sample Ratio U-2341238 = 1.0 Batch: 4176037 RICHRC5011 Work Order: M36EJ1AA Report DB ID: 9M36EJ10 Th-228 2.08E-08 u 2.4E-08 2.4E-08 3.27E-08 uCi/Sample 24% 0.64 7/24/14 03:49 a 1.0 0.98916 ALP127 1.25E-08 3.00E-15 (1.7) Sample Sample Th-230 1.47E-07 6.0E-08 6.5E-08 4.79E-08 uCi/Sample 24% (3.1) 7/24/14 03:49 a 1.0 0.98916 ALP127 1.83E-08 3.00E-15 (4.6) Sample Sample Th-232 5.57E-09 u 1.2E-08 1.2E-08 1.51 E-08 uCi/Sample 24% 0.37 7/24/14 03:49 a 1.0 0.98916 ALP127 8.28E-09 3.00E-15 0.93 Sample Sample ---- Batch: 4176039 RL-RA-001 Work Order: M36EJ1AC Report DB ID: 9M36EJ10 Ra-226 2.65E-07 7.6E-08 9.6E-08 1.02E-07 uCi/sample 66% (2.6) 8/21/14 08:17 p 1.0 0.9892 ASCMAD 4.79E-08 9.00E-14 (5.5) g g No. of Results: 7 Comments: TestAmerica Inc MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.3.3 A2002 11 of 16 FORM I Date: 22-Aug-14 SAMPLE RESULTS Lab Name: TestAmerica Inc SDG: 48381 Collection Date: 6/17/2014 1:00:00 PM Lot-Sample No.: J4F240448-3 Report No.: 61895 Received Date: 6/24/201410:40:00 AM Client Sample ID: R2 SYC Scrubber filter(6208)an COC No.: Matrix: SOLID Ordered by Client Sample 10, Batch No. Result Count Total MDL, Rpt Unit, Yield Rst/MDL, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Prep Date Size Size Detector Batch: 4176035 FFSR Work Order: M36EK2AE Report DB ID: 9M36EK20 U-234 7.92E-06 1.3E-06 2.4E-06 3.28E-07 uCi/Sample 12% (24.2) 7/24/14 03:06 p 1.0 1.0 ALP1 8.99E-08 9.00E-15 (6.7) Sample Sample U-235 5.02E-07 3.2E-07 3.5E-07 2.33E-07 uCi/Sample 12% (2,2) 7/24/14 03:06 p 1.0 1.0 ALP1 5.67E-08 9.00E-15 (2.9) Sample Sample U-238 8.35E-06 1.3E-06 2.5E-06 2.54E-07 uCi/Sample 12% (32.8) 7/24/14 03:06 p 1.0 1.0 ALP1 6.39E-08 9.00E-15 (6.8) Sample Sample Ratio U-2341238 = 0.9 Batch: 4176037 RICHRC5011 Work Order: M36EK1AA Report DB ID: 9M36EK1 0 Th-228 2.69E-09 u 1.1 E-08 1.1 E-08 2.63E-08 uCi/Sample 41% 0.1 7/24/14 03:50 a 1.0 0.98665 ALP128 1.00E-08 3.00E-15 0.51 Sample Sample Th-230 2.25E-07 5.5E-08 6.2E-08 2.79E-08 uCi/Sample 41% (8.1) 7/24/14 03:50 a 1.0 0.98665 ALP128 1.07E-08 3.00E-15 (7.2) Sample Sample Th-232 2.14E-08 1.7E-08 1.8E-08 1.84E-08 uCi/Sample 41% (1.2) 7/24/14 03:50 a 1.0 0.98665 ALP128 7.03E-09 3.00E-15 (2.4) Sample Sample -- Batch: 4176039 RL-RA-001 Work Order: M36EK1AC Report DB ID: 9M36EK10 Ra-226 2.64E-07 6.2E-08 9.5E-08 7.93E-08 uCi/sample 91% (3.3) 8/21/14 08:18 p 1.0 0.9866 ASCKMF 3.74E-08 9.00E-14 (5.5) 9 9 No. of Results: 7 Comments: TestAmerica Inc MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.3.3 A2002 12 of 16 FORM II Date: 22-Aug-14 BLANK RESULTS Lab Name: TestAmerica Inc SDG: 48381 Matrix: SOLID Report No.: 61895 Count Total MDL, Rpt Unit, Rst/MDL, Analysis, Total Sa Aliquot Primary Parameter Result Qual Error ( 2 s) Uncert( 2 s) Lc CRDL Yield Rst!TotUcert Prep Date Size Size Detector Batch: 4176039 RL-RA-001 Work Order: M36K41AA Report DB ID: M36K41AB Ra-226 2.99E-10 u 2.2E-10 2.3E-10 3.41E-10 uCi/sample 93% 0.88 8/21/14 08:18 p 1.0 202.11 ASCLMD 1.60E-10 9.00E-14 (2.6) 9 9 Batch: 4176035 FFSR Work Order: M36KT2AA Report DB ID: M36KT2AB U-234 2.05E-08 u 9.0E-08 9.0E-08 2.23E-07 uCi!Sample 45% 0.09 7/24/14 03:06 p 0.25 0.25 ALP3 7.39E-08 9.00E-15 0.45 Sample Sample U-235 3.26E-08 u 5.3E-08 5.4E-08 1.11 E-07 uCi/Sample 45% 0.29 7/24/14 03:06 p 0.25 0.25 ALP3 3.27E-08 9.00E-15 (1.2) Sample Sample U-238 9.14E-08 u 1.0E-07 1.0E-07 1.98E-07 uCi!Sample 45% 0.46 7/24/14 03:06 p 0.25 0.25 ALP3 6.45E-08 9.00E-15 (1.8) Sample Sample Ratio U-2341238 = 0.2 Batch: 4176037 RICHRC5011 Work Order: M36K11AA Report DB ID: M36K11AB Th-228 1.02E-10 u 1.3E-10 1.3E-10 2.10E-10 uCi/Sample 31% 0.49 7/24/14 03:50 a 1.0 202.11 ALP130 8.02E-11 3.00E-15 (1.6) Sample Sample Th-230 7.53E-10 2.8E-10 3.1E-10 7.04E-11 uCi/Sample 31% (10.7) 7/24/14 03:50 a 10 202.11 ALP130 3.86E-11 3.00E-15 (4.9) Sample Sample Th-232 4.16E-11 u 7.6E-11 7.7E-11 1.47E-10 uCi/Sample 31% 0.28 7/24/14 03:50 a 1.0 202.11 ALP130 5.62E-11 3.00E-15 (1.1) Sample Sample Batch: 4176037 RICHRC5011 Work Order: M36K12AA Report DB ID: M36K12AB Th-228 -2.87E-11 u 7.7E-11 7.7E-11 2.66E-10 uCi!Sample 26% -0.11 7/31/14 02:17 a 1.0 202.11 ALP126 1.02E-10 3.00E-15 -0.74 Sample Sample No. of Results: 8 Comments: TestAmerica Inc MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchBiank U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.3.3 A2002 13 of 16 Lab Name: TestAmerica Inc Matrix: SOLID Count Parameter Result Qual Error ( 2 s) Batch: 4176039 RL-RA-001 Ra-226 4.15E-08 1.2E-09 Batch: 4176035 FFSR U-234 7.54E-07 1.5E-07 U-238 9.78E-07 1.7E-07 Batch: 4176037 RICHRC5011 Th-230 1.11E-08 6.0E-10 No. of Results: 4 Comments: Total Uncert( 2 s) MDL FORM II LCS RESULTS Report Unit Yield Expected Expected Uncert Work Order: M36K41AC Report DB ID: M36K41CS 8.5E-09 4.04E-10 uCi/sample 100% 5.02E-08 5.10E-10 Rec Limits: 75 125 Work Order: M36KT1AC Report DB ID: M36KT1CS 2.1E-07 2.84E-08 uCi/Sample 81% 9.84E-07 3.05E-08 Rec Limits: 75 125 2.6E-07 3.99E-08 uCi/Sample 81% 1.03E-06 3.20E-08 Rec Limits: 75 125 Work Order: M36K11AC Report DB ID: M36K11 CS 1.7E-09 2.19E-11 uCi/Sample 79% 1.14E-08 1.18E-10 Rec Limits: 75 125 TestAmerica Inc Bias -(Result/Expected)-1 as defined by ANSI N13.30. rptSTLRchlcs V5.3.3 A2002 Date: 22-Aug-14 SDG: 48381 Report No.: 61895 Recovery, Analysis, Aliquot Primary Bias Prep Date Size Detector 83% 8/21/14 08:18 p 199.96 ASCNMA -0.2 g 77% 7/15/14 10:06 p 0.26 ALP12 -0.2 Sample 95% 7/15/14 10:06 p 0.26 ALP12 -0.1 Sample 98% 7/24/14 03:51 a 199.96 ALP131 0.0 Sample 14 of 16 (.n !a, ..... 0) Custody Record 'W..;.l24(11l0?) Cl/Qflf Tetco Aetressl 391 East 620 South -CilY . ~~-IZ(DC¥e American Fork ~ Ut 84003 -. . .. ~. --~~--------' Energy Fuels 2014 2nd Quarter Gontrcct/PtJn:JJase OJWI'fOlKJ<e No. Sample f. D. No. and Description Date (Containers for each sample may be combined on osj!l/JOO) [ R1 Dryer BH filter (6207) and beaker .ll 6/17/JM<f R1 SYC Scrubber filter (6206) and beaker 6/16,17/14 . ! R2-SYC Scr~b~er fl_!.ter (6208) and beaker . 6/17,18/14 I R1 Grizzly filter {6210) and beaker -' • J 6/18/14 . .--·---·- l L i -~-.. --1 ·-. - Temperature on Receipt __ _ Test America Drinking Water? Yes 0 ·No 0 THE LEADER IN ENViRONMENTAL TESTING P..mire.9fM?J]f,lSlf![ _ _ __ ---··----·· -~------- Dean Kit!;.hen l.6i.1912 Ol 9: =~:;:~;aCodevrax.r:r~L-.-----l.2b Nu/rJier J~e Crotact.. __ -. ---i Lab Con!acl Analysis (Attach list if Scott Christensen, GaJT~n Palmer more space is needed} I ·-~rM'aytJ//1 Number I Containers & Matrix Preservatives J ~ ... ~ "' ~ N ,; "' ... ~ ~ l! I'! 0 ., "' 'bi§ .. Time g -g ~I ... "' Q ~ ~ I 1-' : !! ·" ~ § ~ ~ ~~ "< 0) 0) 10:00 ·' X1 X 'x X I '!X 8:00 l xj X x 1 I ' .K X 13:00 -, I .X~ I -~x ; 2cl x I I -... I I 8:00 ! X X X I I I l I I I I I ~\..\~d--U.D\..\4'/. '3\:)\s--~ '1:?.:§b\ ·~ iJ-0. ~-""-' rCJraiocf~Number l Page I of _j__ Special lnstiUctionSI Concflfions of Receipt vY\ 7:> \.e ~ \\ -~V'i~ \.o f:(\ I '(Y'-.~~·~ 'M ~\...o .k:. L. I ! 1\1111 ~lllllllllllllllllllllll J4 240448 .. ·- ----•!..:J'._ t . .l --1.1..1--.0.:~-~c:-'""--'""'·nl -;..J 0 Non-Hazard 0 Flammable 0 Skin Irritant 0Poison8 0 Unknovm I 0 Return To Client (A fee may be assessea if samples are retained 0 Disposal By Lab 0 Archive For ___ Months longsr than 1 month) ~ 8eqlii~ (Spgi;ify) 0 T Days 0 14 Days 0 21 Days ~Jn . \C)4C ~ '-'J f''-l<-... i.D-~'4-''\ 2. .,_ 3. Rdmqv!shed By ~Is --·-·-· ·---··---When Co~ete_Email to: Dean or Paul,_ ~tco@tetco-ut.com _ tJiSTRIBVTION:WrllTE-R.e!umed to aieiit<'tirn R~ cANARY-Stay.< •vi/fl~the $8ITij){ef F'IN((~--t'fiir(f"Ccpy Test America !+'+§-. Samffie Check-in List THE I. EADER IN ENVIRONMENTAL TESTIN9 J I .._ ... I lti-JD y ~;;f..t-\'-t Date/Time Received :_,~"4Jc..f .J.ttn f.(>'"'t.~ Co~falner OM Screen 1 estllt (Airlock) (9 () ~pm Initials[ 6=-] I SaJ:Ilple GM Scl·een l{.e-suh ( ample Receiving) -Ej)__ cpm lnilials[ f=-) Client:_s)~ SDG#: \_\C£,~"(\ SAF #: NA~J Lot Number: ~ \...\.. ( d. \..lt:)L\ '-\ cj Chain of Custody# 0 !-!~'--· ------------------------------- Shipping Container ID or Air Bill Number : _____________ NA ~] Yes~ ) Continue with 1 through 4. Initial appropriate response. No [\ ] Go to 5, add comment to #16. Samples received inside shipping container/cooler/box Ye [ ] No [ No Custody Seal \tp] Yes [ ] No [ No Custody Seal [~] °C NA ~) N~~ Wet[ ] D1y[ ] 1. Custody Seals on shipping container intact? 2. Custody Seals dated and signed? 3. Cooler temperature: 4. Vermiculite/packing materials is Item 5 through 16 for samples. Initial appropriate response. ~ 5. Chain of Custody record present? Yes L :\" ] No [ ] 6. Number of samples received (Each sample may contain multiple bottles):,__t.f~-------------- 7. Containers received: lfv f,'f fey ; 4 'l(J ·c..:QV\' 8. 9. 10. 11. 12. 13. 14. 15. 16. Sample holding times exceeded? NA [ ] Yes [ ] No [ , ] Samples have: __ tape __ hazard labels ~custody seals ~ appropriate sample'labels Matrix: ___ A (FLT, Wipe, Solid, Soil) __ I (Water) 'S (Air, Niosh 74~ __ T (Biological, Ni-63) Samples: ~are in good condition __ are leaking __ are broken -.l--have air bubbles (Only for samples requiring no head space) __ Ot~r Sample pH appropriate for analysis requested Yes [ ] No [ ] NA . ] (If acidification is necessary go to pH area & document sample ID, initial pH, amount~· 3 a.dded and pH after nddltlM .. on table) Were any anomalies identified in sample receipt? Yes [ ] No LY ] Description of anomalies (include sample numbers): NA ~ ] ------------------- Sample Location, Sample Collector Listed on COC? * *For documentation only. No corrective action needed. Yes [ Additional Information:~l-'-'---~----.---.--.-------..----.--=--...,.....--=-"'---,~-~-----~- ] Client/Courier denied temperature check. ] Client/Courier unpack cooler. LS-023 Rev. 17, 05/13 Page 1 ofJ 16 of 16 APPENDIX D South Yellow Cake Scrubber Figure 1. Facility Schematic Representation Yell ow Cake Dryer Baghouse Figure 2. Facility Schematic Representation Grizzly Baghouse Figure 3. Facility Schematic Representation Production and Control Equipment Data South Yellow Cake (Scrubber Flow Rates) Yellow Cake Dryer Baghouse (Delta P readings on Field Data Sheets) Grizzly (tph of material and belt speed) D Fadl;ty Energy Fuels Resources t a t y Stack Identification: South yell ow Cake Scrubber l+--0~1 ~ a: Distance upstream from next disturbance, feet 7' ------------------ ~: Distance downstream from last disturbance, feet 30' y: Distance of Sample Level to Ground, feet 65' 0: Stack Inside Diameter, inches 1 :2_75" ------------------ Estimated Moisture, percent 4-8 100-120 Estimated Temperature, °F ------------------ 3.000 Estimated Velocity, fpm _______________ __ Control Unit Type: Scrubber Number of Ports 2 ~ Figure I. Facility Schematic Representation Process Type: Yellow Cake Processing Fao;,;,y Energy Fuels Resources t a t y Stack Identification: ·yell ow Cal(e Dryer Bagh.ouse l+--0--+ I ~ a: Distance upstream from next disturbance, inches 57 H ----------------- ~: Distance downstream fi·om last disturbance, inches 454" y: Distance of Sample Level to Ground, feet 65' 0: Stack Inside Diameter, inches 16" -------------------- Estimated Moisture, percent 0-:?% 125 Estimated Temperature, °F ----------------- Estimated Velocity, fpm 1.400 Control Unit Type: Baghouse Number of Ports 2 <(' Figure 2. Facility Schematic Representation Process Type: Y e!!mv Cake Processing F•cH;ty, Energy Fuels Resources t a t y Stack Identification: Grizzly B agh 0 use 1~0~1 p a: Distance upstream from next disturbance, inches '4.5" ----------------- 0: Distance downstream from last disturbance, inches 48'' y: Distance of Sample Level to Ground, feet 28' ------------------ 0: Stack Inside Diameter, inches 1?:75" ----------------- Estimated Moisture, percent 1% Estimated Temperature, °F Ambient 775 Estimated Velocity, fpm ______________ _ Number of Ports 2 Process Type: Control Unit Type: r--..1.---------IOre Unloading and Conveying <f l:3aghousc Figure 3. Facility Schematic Representation .. L Energy Fuels ~soulces, Blanding, UT Process Data tj.,,__.. I I Source: South Yel;ow Cake Date: [}t(~ { L/ : ..: /.-lf._. Time /If 'l t) I'~ ~ i> I r / ·-::-'_-:: ( t ·~ ~ ' ... I '1/.· -·) r -. ;.... .. i~ " ) c.. )D I ·~ ._/ Scrubber Flow GPM #1 #2 L1P ' l ·) -(3 + • ll . l .. <7-1 ,/-__, /?p 1- > 7 /1 \ .. ....... -..-1 ~ . · . ...:; ---,!...., • --/ ~-I --/ v '--._/ ~~-/ ' ·--c--1 ( "-:-• - / ;) ~ ( (!.--,.) ~ --:) ~-......-' < ( ~ ·-( ~ ,-t -(~ -,_ ~j-l/ '/ )" '? -l. . { 1 -~ :; 2'. u ..,. ,.., 1 ,' --~ 2. z__ ~ . .-- / ·-. '-. ./ .2, 7 . \ / -I ~- 'I. ") -~ . ~I ) ) 2. I.J ·; ( l. { 1-s- J I f ~-·{ ~i ,' l -t-,..-,....._ ) -' l~.c;- 1--"¥ :;.~ ~z ./ / .t>\ 1' ~--') -/ .. I ·.·( . --.::., J_ ~ ~ I \ \ '.:.. :.· ... ~ . .. • f .. Energy F~ls Resources, Blanding, UT Process Data fl. 7 '-"'f_.-_ -' Source: South Yellow Cake Date: G1t+~(4 Scrubber Flow GPM Time #1 #2 ~p Uj :~~ 3.'L 1·~ 3/-~ 1 <=i. '9. s,- , $.: t..{ 5!:7 ). ) 7·'-/ 3z.o 2o. oo !Sf; l~ 5 .z._ 1.5,-3 2. ( t "l. '\ ...S'- l'f _. <-i.S 5 ·Z. -:J ·s-5-l--~a I <=t .7; 1 s~: ts-1;.1._ .1· ~ ~~ ·'1 I""-, f- 1 s~; L(.,~-3 .z_ l·~ 3\ -~ zo-o> ,c.:..ts-+·~ ) {· ~ Z D· o o '?· "t.- ll;'-ts-1·Z-i·<J" .?! . s. {~.'1'1 n-: ~~-3' l ;r.~ 3t-1 fl. g _) . roo s·+ 1·) 7l·s (S,. ( D ~so s· r ~-'Z.. 3 1 . )-·. t ~-'1 D OJ;oo ?·y r:J-~ ~ \ .L( I 4 · ""l s-- '1:3o 'S-· ~ 1·( )\· ~ '10,..) j"O! ll D $·~ 1~ 3!·y 11.. qo ~a; 30 ),q lO ?2·0 1'\.ov ·. ~. 1 (: 0 0 5· v; l.l 3' ·4 It-Is- 1/: > 0 )·0 1·0 )2· u 1'1 .( z .. , z_: 0 0 ~, 'l5 1 ~~ ~ (-C, I~, \ D ll:)D ~·v 9·D ~~-~ 1~·2) 13 .. . c)O Energy Fuels Resources, Blanding, UT Process Data jt. . Source: Grizzly Baghouse Date: 'ltB f lt.(_ . Time Tons (Integrator) tph fpm 0'.19 ~ 3 58oo ' (.., cJ l( l, 6 e:t.t li (, 5S815 3'2..0 \It·~ \ ·. ( PJ "'358 3 J \L./),.,-t~L '-I 1~44 -~558So It-t { l tL ~ i()'.\1 (p~5870 3~ lll· 4 10 '.Lf q ~ ") 5 58) 7_0 I l (. ~ \ } t. 2-L-~ ).5 ~ o8 Lt~ t t( .-q- \t:L--t~ ~ 7 (910 L{) tllt'::f- l~'-L 3 G,'!> Sq2--(" t_l:) 1115 ~z:qc:r / [p)5~3) y{ l t(. s \ ~ ~ 2l ~ 3 S<=t 5o 3o \((·:> 1-:):iPJ (cJ) 59 b) Zo lllri t '-{ '. ?..2-"3 59 B r z_o ,/ {{{,j 1'-t', )O (p)(,U)00 yl( pl.-)' l5'. 2.-'2-(., ';:)~ b "LO 3S \ llr ~ \ 5 ~~ { ~"3G. Q)O 2) lll, 0 ~· / l · I) lo)G, e'1~ lS l u '(p - APPENDIXE Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature sensors were carried out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 4 Schematic of Method 5/114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-test Dry Gas Meter Calibration Data Forms Type S Pitot Tube Inspection Data Sample Box Temperature Sensor Calibration E Temperature Sensor t ~Probe ~ TypeS Pitot Tube Temperature Temperature Sensor lmpingerTrain Optional, M3YBeReplaced By An Equivalent Condenser l Temperature Sensor Nozzle 1-SE:tT;acect Sensor~ Gooseneck I ~--·---·--------- lmplngers "' ~ "'~~ / TypeS Pitot Tube ~ Stack Wall f--~ I Glass Filter Holder ~ I I Heated Area Manometer Orifice Dry Gas Meter Water Empty Silica Gel Air-Tight Pump Figure 4 Schematic ofMethod 5/114 Sampling Train Vacuum Line Vacuum Gauge METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three Cl'itical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure 3) Run at tested vacuum (from Orifice Calibration Report). for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information 1n the GREEN cells, YELLOW cells are calculated. METER SERIAL .l .. ·--I CRITICAL ORIFICE SET SERIAL et 1453S EQUIPMENT !D #: K' I TESTED ..------r---1 FACTOR I VACUUM 0 G G RUN# I /AVGI I /in Hg) 0.1!113.1 13 l C.S137 13 0.8137 13 0,5317 13 2 0,5317 13 0.5317-1l 0.3307 13 (1.:1307 13 S· 0.3~07 13 261.525 268.512 275.475 3.00JI21 3.06.25.1 312.128 242.1140 248.398 .254.428 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 1U.512 6.987 .. 75 2ZSA75 6,963 •• 76 281.8~8 6.403 69 7Z 306.251 6.230 69 67 312.12.8 5.877 69 sa 311.~40 6.212 69 68 248.198 5.558• !ill 65 154.428 6~030 .. 59 260.240 5.812 s·g &t The followirlf! equations are used to c-Cllculale the 11!andard volumes of air passed through the DGM, V,., (std), and the critical crifice, V:1 (std), and the DGM calibr3~on factor, Y Thesto equations are automaliGally calculated rn the 5preadshaet above 75 n 75 76 71 75 68 " 69 68 71 67 64 sa 70 69 71 75 lis 'NWi1·iiiWM!W.., ~ •... ~?~ -!~·- 1 . . 2014 Pre-calibration INITiAL FtNAL AVG (Pa01) ~ 25.35 IFYVARIAT!ON EXCEEDS 2.00%. ORIFICE SHOULD BE RECAUBRATED ELAPSED I l ;J [rtMEe(MtNII r:;J I I I I ~ 40 80 02 76.75 ~ ~ 5.!683 5.8312 ~ ~ 76.75 0 D 5 84S1 5.8312 !:ill, .l.:.an 76.50 D D. .Y!!!l !d!l! 1:.Q.!U! .Ul!. AV G = .!!.ru :J!4! n 68.00 9.00 1.10 s 2963 5.2758 ~ 1.:lli 7j 69.00 8.50 ~ 4 9827 !!J1! ~ 70 69.00 9.0D llill ~ .!Jm! ~ AVG :c Qa!!! :Q.J..! 70 67.00 1).00 4.7244 4,7397 ~ ~ 71 69.75 1uo 5.p•a• 5.1043 1J!ll LID 76 72.75 13.50 0.40 ~ ~ J..,Q,Ql Llli AVG • .!J!2! !!d!!. AVERAGE DRY GAS METER CALIBRATION FACTOR, y = r:J!iiO I AVERAGE ~H,. .,-1..495 I (1) 1/-mu•.tJ = K, * Vm• l'boi"-l~ ~f3~(1) 't = Net volume of gas sample passed through DGM, corrected to standard conditions K, = 17,64 aRlin. Hg (English) I a 3858 ~Kimm Hg (Melric) (2) (3) v",.t•t" == K '• Pbur * 0 .. ,f!;mh- = Vc~~ .... , Vn1r.rdJ T'" = Absolute DGM avg, temperature COR~ English, oK-Metric) = Volume of gas sample passed through the critical orifice corrected to standard conditions T ~e = Absolute amblenl temperature ('"R-English, ~K • Metnc) K' = A11erage K' ractor from Critical Orifice Calibration = DGM calibration fector Ice Bath Amb1entA1r 8o1JinaWater <~.HI!!= ( D.75 e )2 dH (Vm(std)) V~(std) Vm Temperature SensorS Reference In Out 'F 'F 'F 33 62 202 33 62 203 33 62 203 PRE Console #4 Calibralian 2014 ---"is ""'"*""'*N'M''MV ~ I -,. 1' ~---, METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range 2) Record barometric pressure before and after calibration procedure, ENVIRONMENTAL SUPPLY COMPANY 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 2014 Pre-Calibration Console 9 4) Record data and informalion in the (~: :J-t. cells, YELLOW cells are calculated, FINAL AVG [P,.,) METER SERIAL #:1 '·-· ---~-I CRITICAL ORIFICE SET SERIAL#: 1453~ EQUIPMENT ID #: I 25.45 I 25.45 IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATEO K' TESTED .-----:---~ FACTOR I VACUUM 0 G G RUN# I (AVG) 0.8137 0.8137 0.8137 0,5317 2 0.5317 0,5317 0.3307 2 0.3307 0.3307 (in Hg} 12 12 12 12 12. 12 12 12 12 88.612 94.007 99.367 105.106. 110,310 115.871! 121.2-05 126.327 131.458 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 94.007 99.387 104.803 110.310 115.878 121.084 126.327 UL458 1J7,053 5.395 5.380 5.416 5.204 5.568 5.206 5.122 5.131 5.595 65 fi5 65 70 TO 70 n n n ELAPSED D~ TIME (MIN) A~~-I ft ..;..__._..L,;......;..,.;..r, 78 7~ 75 75 79 79 75 75 79 80 75 75 7&.75 5.00 § 4.5541 77.00 5.00 0 4.5393 T7.25 5.00 o 4,5676 4,5203 !Mll 4.5203 lhlli. 4.5203 l!,.lli AVG= .!hill. 75 76 69 71 72.75 7.50 4.4031 4.4097 ll!!! 76 78 71 71 74,00 8.00 4.70 4 703& 1.QQ1 78 80 71 71 75.00 7.50 1.20 4.3862 ~ .1....I!M AVG= ,!,QQI n!n " n niR n n J& In n n 73.75 12,00 § 4.3161 74.00 12.00 44 4.3217 74.00 13.00 .44 ~ ~ L.!!ll ~ 1.Qll ~ .1..22! AVG= .1..l!11. The following equations are used to calculate the standard volumes of air passed through the DGM, V m (std), and the critical orifice, V ~ (sld), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 1.002 J (1) (2) (3) i 'm,.,,;, = K, • ~-111 • Pb(lr+(AH 113 61 Tm I1cr .rc/; :; l)har * e K'• -Jn;;," = Net volume of gas sample passed through DGM, corrected to standard conditions K1 = 17.64 'R/in. Hg (English), o 3656 'Kimm HQ (Metnc) T m = Absolute DGM avg temperature (c:R ~ English, °K-Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T111"b = Absolute ambient temperature ("R-English,~-Metric) K' = Average K' factor from Critical Orifice Calibration Vcr~~IJ, l"= --= DGM calibration factor Vrn,,,,J; AVERAGE llHe =r 1 .ssz 1 z .!!Hi!!!= ( 0.75 !l ) .!!H (Vm(std)) V01(std) Vm Temperature Senson; Reference In Out "F 32 72 201 "F 33 73 202 "F 33 73 203 l ::!!,!!§. .Q.,ll (1.94 1.743 ug 1,741 1.652 1M!!. 1.6'!5 1.565 1.565 1.565 Console 9 Pre-test 2014 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. b \!""'"• \',n,., llrll.tl>ll•o~4 -~i,~_-, 3) Run at tested vacuum (from Orifice Calibration Report). for a period of time necessary to achieve a minimum total volume of 5 cubic feet 4) Record data and information in the GREEN cells, YELLOW cells are calculated, DAre:! ...... y,. I METER PART~ Conoole 4 METER SERIAL #;I .. DDO I CRITICAL ORIFICE SET SERIAL#: 14535 EQUIPMENT ID #: K' TESTED FACTOR I VACUUM RUN II (AVG) Qn Hg] 0 G G 0,8137 0.9137 0.8137 13 13 13 § .o I I T r -11 I I I .0 .0 0.5317 13 21U04 -217.:!&5 z 0.5317 13 217.365 222.939 0.5317 13 222.!139 228.520 z 0.3307 ·p 0.3307 13 0.3307 13 § USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 5.561 5.574 5.581 .o .o .o M ~ ~ ~ n ~ ~ ro n n ~ ro ro n n I I lll-11 DGM AVG 0 0.00 72.75 73.25 73.50 0,00 o.oo o.oo FINAL AVG (P .. ,) I 25~55 I ELAPSED TIME (MIN) e 25.55 §§ § a 00 §§ ilm 4.7268 .um. Energy Fuels SYC Dryer IF YVARJATION EXCEEDS 2.00o/o, ORIFICE SHOULD BE RECALIBRATED l AVG= 4.7311 1.002 4.7311 1.000 4.7311 1.000 AVG= 1.001 ~ AVG ~ ~ MQQ The following equations are used to calculatethesta11dard volumes of air passed through the DGM, v. (sld), and the critical orifice, V0 (sld), and the DGM calibration factor, Y. These equalions are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 1.001 I (1) (2} (3) Vm,,,,; = K,•l'm• l'hot· .. (~/1 11~.61 1'111 = Net volume oi gas sample passed through DGM. corrected to standard conditions K, = 17 64 'Riin Hg (English), 0 3656 'Kimm Hg (Metric) T m = Absolute OGM avg temperature (0R -English, °K-Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T;meo-= Absolute ambient temperature tR-English, °K-Melric) K' =-Average K' factor from Critical On free Calibration V'ct;\r.l) f-----= DGM calibration factor -Vm1,:J, Ice B~th Ambient Air Bmhng Weter AVERAGE .<1HC!! =c:!501 :J &H@ = ( 0.75 E! )~ AH (Vm(std)) V.,(std) Vm Temperature Sensors Reference In Out OF 33 62 202 OF OF 33 62 203 33 62 203 POST-TEST Console #4 Calibration 2014 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES '.:S --·~, ·..,.';~ r- 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. ENVIRONMENTAL SUPPLY COMPANY 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet 4) Record data and information in the C-! ::'·Fe\ cells, YELLOW cells are calculated FINAL AVG (P.,,) Energy Fuels Dryer Baghouse DATE:' ....... .• I METER PART#: Console 9 METER SERIAL If:' ·--· -~-I CRITICAL ORIFICE SET SERIAL ll: . 14535 I 25.55 I 25.55 EQUIPMENT ID #: IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED K' TESTED FACTOR !VACUUM RUN# (AVG) (in Hg) G: 0.5317 13 0.5317 13 0.5317 13 833.506 838.984 838.984 844.124 844.124 849.259 D:EB EB o:rn EB USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 5.478 5.140 5.135 .0 .0 .o .o .0 .0 72 69 72 56 67 72 72 75 67 68 72 75 75 liS 58 I I I I I I I I I I I I I ELAPSED ::1 TIME (MIN) ~9--~~~~~~~ 68.50 ~ 4.7019 70.60 0 4.3962 71.50 0 4.3826 0.00 §§ 0.00 0.00 :::PH 0.00 bD 4.7132 .tm 4.4186 .t.!!Q§. 4.4186 1.00B AVG= .t.!!Q§. AVG= AVG= The following equations are used to calculate the standard volumes of air passed through the DGM, Vm (sld). and the critical orifice. V" (sld), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 1.005 -, (1) r·m,,,,, = K, * Vm• ?bar+ (M-f /13.6) Tm = Net volume of gas sample passed through DGM, corrected to standard conditions K1 = 17,64 'Riin Hg (English), 0 3858 'Kimm Hg (Metric) AVERAGE ~H1'1 =r 2.843 , l'har * e f/cri.''·'· = K'*-...Jl~rnh T m = Absolute DGM avg temperature ('R -English, 'K-Metric) 2 t.H~= ( 0.75 e) ~H (V.,(std)) V0,(std) Vm (2) (3) Vc~•rdr l' = _--~m\lld) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T,mb = Absolute ambient temperature i'R-English, 'K-Metric) K' = Average K' factor from Critical Orifice Calibration = DGM calibration factor Temperature Sensors Reference In Out 'F 32 72 201 'F 33 73 202 OF 33 73 203 1 !!J!Q 2.862 2.841 k.ill Console 9 Post-test 2014 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet 4) Record data and information in the U'"-" :-;cells, YELLOW cells are calculated. METER SERIAL II:! ····--·-I CRITICAL ORIFICE SET SERIAL II: 145JS EQUIPMENT ID #: K' TESTED FACTOR VACUUM l ORIFICE II ) RUN# (AVG) (in Hg) 0: 0.6808 13 0.6808 13 0.6808 13 INITIAL FINAL 814.600 820.406 820.405 827.109 827.109 832.485 5.805 6.704 5.376 68 76 68 79 68 80 7~ 63 80 $3 U1 85 63 65 66 D:EBE D:EBE .0 .0 .0 I I I I I I .0 I -~-I I I I .0 .0 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: The following equations are used to calculate the standard volumes of air passed through the DGM, V m (sld), and the critical orifice. Va (std), and the DGM calibration factor, Y These equalions are automatically calculated in the spreadsheet above DGM AVG 70.25 71.75 73.00 0.00 0.00 0.00 0.00 0.00 0.00 2~ :l -··~i---•.:~ *fflli&IMI#i1Ppiffli!M1!.W 1· • -- ENVIRONMENTAL SUPPLY COMPANY ~ AVG(P._,) I 25.65 I 25.55 ELAPSED TIME(MIN) 9 §§.05 _ 2.05 2.05 §§ §§ ~ Hill 4.5754 Energy Fuels Grizzly IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 1 (3) J y Y VARIATION(%) 4.9219 0.991 5.6791 0.993 ~ Q,ID AVG= 0.992 2d!Q AVG= AVG= AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 0.992 I AVERAGE <loH~ =I 1.716 I (1) r··m""" = K, *I'm* Pbar+(J}.H /13.6) Tm = Net volume of gas sample passed through DGM. corrected to standard conditions K1 = 17 64 'Rtin. Hg (English). o 3858 'Ktmm Hg (Metric) (2) (3) Vc.~,~: ,~.,,, = K '* l)har * 0 .J'J'wnh Vc'(j/,,j r = . --~ /11t \I;/: T rn = Absolute DGM avg temperature ('R -English, 'K-Metric) = Volume of gas sample passed through the critical orifice. corrected to standard conditions T,""' = Absolute ambienltemperaiUre ('R · English, 'K ·Metric) K' = Average K: factor from Critical Orifice Calibration = DGM calibration factor 6H® = ( 0. 75 e )z 6H (V m(std)) Vcr(std) Vm Temperature Sensors Reference In Out 'F 32 72 201 'F 33 73 202 'F 33 73 203 1ll!! 1.7]6 gg Console 9 Post-test 2014 Type S Pi tot Tube Inspection Dattt Date: _):....:l...:..l _tl.-__:{~13 __ _ Pitot Tube Identification: __ 2._\ --------- Technician: __ M_._;,IY\_..:~:....:':....~...:o..M:..:::...;....::C\..:.::::.:..(...:t.A..::....::. _____ _ r)~ ~ --"/v Dt~ '31) ill, Is 1\ = P0 ? Is 1.05 • D, s D, $ 1.50 • D,? Y-eS PA= • { 2-)-in 2 ? B ........-( a, I ~a: z: -;~- ~ .. -.. --·r· w --""'"~ -··-··-··-~· ··--~ F '" _ ... ! .. CF:IJ , I ,. L. -(' Pn= ,") rt1 <tO" n,< !0° llr < .S" p, < 5" Z :S 0.125 in W s 0 03125 in. W > 3 i11chcs Z > 3/4 inch 1\. u.~ D 0 aJ ~ z... p,= 0 p, = Z"-,\)18 ln. W = ' 0\ Lf in \Y -~c.r In, Z= '\ Ill. •"·~ ~-·r-----y <': 3 inches ,,, Y = ______ in. Th•• pi tot tube 1\lects the specifications for a calibration factor ofO 84? Tempernturc Sensor Calibrnt1on Reference· ·;' ... Temperature Tcmncrnltll\! Temperature .. !';. ' ... -;.;·~ Source Reference Sensor Ditlhence IMediulll) rn ("I') <"fl AIR (, 8 (,'1 I Probe Continuity '{e ~ tleat Check 248 \[(.) l.~ 0 AIR (.,~ <..6 0 ICE WATER ~~ 3 Ll l Stack BOIL WATER 2~l. 2.o L. I SILICONE OIL . Type S Pitot Tube Inspection Data Date:_\~l-_/_I'Z-_____:__;/1...;:.)_ Pilot Tube Jdentification: __ "Z_T.:........·_....:\ _______ _ (I Technician: /V\ • M S rJCI.,Mil,./ (,)-.... Dt=_:} )O __ in ls P A = Pa ? '( ~.s __..;. ______ _ .:..l'.t;.,_=_·_?.=-1.....:)_~~----in . ls 1.05 • D, s D, ~ 1.50 • D, '? _"/...!.-2:-e..::...}~----- .:..1'-'"B-~_._z..._{._)_"" _____ in -o -'d -~~-·~.w ............. -r... ,., . ·~ a,< 10° a2 < 10" fl, < 5" lh <5'' Z~0.\25 in ~ !'' ........... (:) ·~ ~:.~ ~;~ 1-·"""" ·--::--~---Y::0:3 inches . . a, "'--=0;.._ ___ ·0 · U) "' __ "2..;:_ __ _ p,= __ .=,.3 __ _ p,= _____ _ . o!l( Z= ------in. _...;,.. _ ___._ __ ln. -----'------'" Y = --~::.:...:,'2::.. • .:...·(_'_in lhe pitot tube meets the spccilications for n calibration factor of0.84? '{e) "I'CIII(!CIUlurc Sfur$11r C~lihr1111011 '-: .~.4t Temperature TelllO<\tntur~ Ttmpomture ~ . ' Source Refetem~c Sensor Dilkr~nce t,,~· ~~ (Medium) (''F) (UF) ("Fl AIR II 17... I Probe Continuity '(-<:~ 11cat Check 248 'kS 2.)0 AIR Co cl "l 0 I TCEWATER ~ .3 11 I Stack BOIL WATER (oL <..o \ I SILICONE OIL Type S Pito! Tube Inspection Data Dale: _ __:_1"1..___:_/1_~_/_1_3 Pi tot Tube ldenlification: _ _::.3~B~-~~(;.,.·7::__ _____ _ Technician: _,_v_\:....._...JM!....-l--=~"-'NL:. ~o..:=vV\.-=.....:~v....:....:...(_v--,;___:_ ____ _ l Pl. t P(l Dt= .~f-) ln. PA = .1..\{po in lsP"=Pn? 'f~> __ ,;,.__ __ _ ls 1.05 • D1 ~ D1 ~ 1.50 • D1 ? __ '(:._4.:..:~~---- Ps = I 1..11o t> in a 1 < 10" a,= u 2 < to• o.l= ~1= __ 1. __ _ ~' < s• ~,= __ .J __ ~ -] -• ol~ z Z :-; 0 125 in Z= in. ? ( _ ........ ~ ~0?FA·:=r.-~~. w \V:;; 0.01125 in W= ·ooB in W > 3 inehes w~ ~ in~ Z > 3/4 inch Z= 3/c..i in The pilot lube meets the specifications for a c.11ibration factor ofO 84? \IQ.S Temperature Sensor Cnlibrntion Reference· ''\\ .,._ -.' Temperahlre Temperature T~!11(1ei'Ol1UIO: !~ ·'~ SClurte Reference Sensor Difference ., ..... ~ .. (Medium) ("F) (vF) C"l·l AJR r...<o (,1-\ Probe ContinuitY \I~~ Heat Check 248 '-ro ~-e..':; AlR lo+ (,~ I ICE WATER 3'i 3'1 0 Stack BOlL WATER 2.0 ~ 1.~3 l SILl CONE OIL TETCO Sample Box Temperature Sensor Calibration Date: 12/13/13 Calibrator: Dean Kitchen Reterence: Ome~o~a CL3512A Thermocouple Temperature Temperature Temperature lJnit ID Location Source Reference Sensor l)ifference (Mctlium) ("F) ("F) ("F) Oven Water 32 34 2 Water 204 203 -I A Oven (4) Water 33 34 1 Water 204 202 -2 Impinger Out Water 33 34 I Water 204 203 -I Oven Water 33 33 0 Water 204 202 -2 B Oven (4) Water 33 34 I Water 203 203 0 lrnpinger Out Water 32 33 1 Water 204 202 -2 Oven Water 32 33 l Water 204 203 -I c Oven (4) Water 33 34 I Water 204 204 0 lmpinger Out Water 33 33 0 Water 203 202 -I Oven Water 33 34 I Water 203 203 0 D Oven (4) Water 33 34 I Water 204 204 0 Water 33 -.-. 0 lmpinger Out .).) Water 204 202 -2 Oven Water 33 3'4 I Water 203 202 -I E Water 33 -.-. 0 Oven (4) .u Water 204 203 -I 1mpinger Out Water 33 34 I Watet· 204 203 1 Oven Water 33 34 I Water 204 202 -2 F Oven (4) Water 33 34 I Water 204 202 -2 lmpinger Out Water 33 33 0 Water 203 202 -I lmpinger Out G Water 33 34 I Water 204 203 -I Impinger Out 1-1 Water 33 34 I Water 204 202 -2 -Water 33 33 0 Impinger Out I Water 204 202 -2 lmpinger Out J Water 33 34 I Water 203 202 -I APPENDIX F The testing followed the same procedures as outlined in previous protocols and tests at this facility. ATTACHMENTH SURFACE WATER GRAPHS AND FIELD DATA SHEETS 1.00E-05 1.00E-06 1.00E-07 -.!! C'CI ~.OOE-08 C) 0 ...J - 1.00E-09 1.00E-10 1.00E-11 •• • • • • ... . -• -- ---:. _, ~--:....._ ------ Ia --- ~ o_,CO'l, ~" ~ ~~Oj ~~ Cottonwood Creek Dissolved Radionuclide Concentrations (uCi/ml) ... -- • • ----- . o_,OJ'), ~" ~rV"' - • -- ........ - • • • • - • • ~ • • .. - • ... .._. __ .._....._ ____ PJCO ':!..~Oj ~ro ~n;, ~ ~ ~" 1----;u:_Nat. • Th-230 • Ra-226 I . ~0; ~ <,j.~Oj .. • .. .. • -.- --r:;)~l>< ~rc ~" r::::,rf' <,j.~rc 1.00E-06 1.00E-07 1.00E-08 -.!! C'CI ~.OOE-09 C) 0 ...J - 1.00E-10 1.00E-11 1.00E-12 fb<t;, ':\to..Oj ~"' Cottonwood Creek Suspended Radionuclide Concentrations (uCi/ml) • ... -• -.. • -• ... --•• • I. ... ~· • • .. ... • .. i ..... .-i . -=-· ... • • • • • ·-· ··--·------·-·-····-----••• • ... .. . . ' ~ 2><::) 2>n;, 2><,;, 2>'0 &)to.. ~ &)co &)<?> to..~ to..Oj Qj to..Qj ~to..Qj ~to..Qj ~ ~ ~ ~ ~ ~ ~to;. ~ ~€)1 ~€)1 ~€)1 ~€)1 ~f); to..rV~ ~to..f;j rJ. n} ~ q}cv <.j."-~ n} to.." [ • U-Nat. • Th-230 • Ra-226 [ * ••• - - to..<,;, ~ ~ ~ ~€)1 ~€)1 rVto.. to..~ 1 0.1 0.01 0.001 0.0001 0.00001 -Cl) ~.000001 C/) tn ~0000001 - 1 E-08 1 E-09 1 E-10 1 E-11 1 E-12 1 E-13 ~r:::,OJ /\,.,r&~ - "r:::, ~ ~<),.'1) Westwater Creek Dissolved Radionuclide Concentrations (uCi/ml) "r:::, fVr:::, c6-"<::j ............ ~ cV~ ...... ...... ~ cy."t:;. ~ ~"<),. ~~~ [ • U-Nat. •Th-230 & Ra-226 J ~"<),. c6-~ ...... r:S-" - ... ...... ~ ~ ~'1) "" ......~ ~ <,j.ro 0.1 0.01 0.001 0.0001 0.00001 -Cl) 11J.000001 en ~000001 ...J - 1 E-08 1 E-09 1 E-10 1 E-11 1 E-12 1 E-13 ~OJ '\\ro Westwater Creek Suspended Radionuclide Concentrations (uCi/ml) ~"~ ~~f)) - ~"~ c8-"~ ':!.."'-" ~~ ~"" cy.~ ~"~ ~~ I • U-Nat • Th 230 • Ra-226 I I ':!.."'-~ ~"co "~ ' ':!.."-0;) <d-ro _._ "1'-."-0;) ~f)) "~ White Mesa Mill -Standard Operating Procedures Book #11: Environmental Protection Manual, Section 2.1 Date: 2/07 Revision: DUSA-1 Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle o~onwood ~estwater Canyon Other (describe). ___ _ DATE: 3/5 I ~0 /~ pHBUFFER 7.0 _7_,_0 ___ _ BY: I"H (Sampler's initials) pH BUFFER 4.0 __ L/!,_. 0 __ _ SPECIFIC CONDUCTIVITY __ 1._.1'--'Cf'---------.....t:uMH==O=s STEAM DEPTH: pHofVVATER __ 7~~~9~l~-------TENW __ ~I=3~.6~1 __ _ . ' COND !!mhos £71 COND !lmhos £8'-f pH Units _7_..!...!.....7'-~=----pH units 7, $55 Temp °C L?,. 7 S Temp °C l~. Sb COND J.tmbos b3Y COND !lmhos t,gL.f pH units 7,SD pH units 7, g 7 Temp °C l'?:>,f:.O Temp °C 13 .SS Conunents: Acr •\lc.J o" ~fi-e a..~ 12.10 G-ro.b 5o-r>1fles. pe,Qrl""'c.J o-.t 12.15 LeG $.-~}c. J-·.\2(7 . _,;tJJ'lC(i Ga-r r1r1 •' Cl~(j otll prc;y:Y'~ White Mesa Mill -Standard Operating Procedures Book #11: Environmental Protection Manual, Section 2.1 Date: 2107 Revision: DUSA-1 Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one):Cononwood Creek('}§Stwater Canyog)Other (describe) ____ _ DATE: 3/5/Z.or'-\ pH BUFFER 7.0 __ /-'-'#=0"------ BY: G-o..r-r-lii\. Po..l-"""c.r { (,.,e. (Sampler's initials) pH BUFFER 4.0 __ 4_,_,_ . .....,0=----- SPECIFIC CONDUCTIVITY _ _.9_.9__,lt.___ _____ -==u=MH=O=s STEAM DEPTH: pHofWATER _____________________ _ TE~--------------- 'I COND cbll=nho=s<---------COND ll=mh=os,__ ______ _ pH Units -------------pH units -------------- Temp °C ____________ _ Temp °C ____________ _ COND ll-=mh=os::.-___ _ COND!.i=mh==os~------- pH units ----------pH units----------- Temp °C ------------Temp °C ___________ _ Comments: Anl J(.·l """ s-a.. c.. I--\ 'Z.'"i y k.-..re· ..... rw-... w L ' L(h¥ p r<S ..... ±. k[Ll b !.o,)L;._( l>ev' p kot,-, .....>.:...I ~~- LR"' .,;; f. c.. t?--1-rZ.-1:h. .3/p=t /I '1 A,.,.,.,,.), l'lb !:;'/L .;.l-IQ('l.). G·w.cd<>i p.:.u;J ~ et-(,::.o.h ~1'2.7/1'-\ L ru:.l<-Wo\.5 J..'"'f , SU. p\..o..ah.!, Arrwc,ol oe= s .±c.. D-.t I Soo. C rr-t \L '-o,.l....S J.."y .. Sc.c, 9 b--o+o. EN:RGY 1_/\0CH:;J\ t C'HI!.___~-. www.enBfEYiab.com A1llltflal £'""'-Slltu 1/BZ Helena, MT 877-472-0711 • Billings, MT 801-735-448! • Casper, WY 888-235-0515 Gillette, WY 816-188-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 March 12, 2014 Energy Fuels Resources (USA) Inc 225 Union Blvd Ste 600 Lakewood, CO 80228-1826 Workorder No.: C14030228 ANALYTICAL SUMMARY REPORT Project Name: 1st Quarter Surface Water 2014 Energy Laboratories, Inc. Casper WY received the following 1 sample for Energy Fuels Resources (USA) Inc on 3/7/2014 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C14030228-001 Cottonwood Creek 03/05/14 12:15 03/07/14 Aqueous Solids, Total Dissolved Solids, Total Suspended The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QAIQC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: 4j'~ c\:k nv',g_____ Report Proofing Specialist Digitally signed by Kathy Hamre Date: 2014.03.12 14:46:12-06:00 Page 1 of? ••·• -••·• -·-_,._ ~,.• __ .,, "' .. ,,,. ........ --· .......... -~r··• •• ...... -·---...~- Gillette, WY 866-688-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218 CLIENT: Energy Fuels Resources (USA) Inc Project: 1st Quarter Surface Water 2014 Report Date: 03/12/14 Sample Delivery Group: C14030228 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r-Energy Laboratories, Inc. -Rapid City, SD eli-cs -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify Ell's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of? EI\ERGY t 1\.-... C•I-id C::',ol: • www.energylab.com Aul1flai~SMIB!2 Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-1515 Gillette, WY 868-188-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 1st Quarter Surface Water 2014 LabiD: C14030228-001 Client Sample ID: Cottonwood Creek Analyses Result Units PHYSICAL PROPERTIES Solids, Total Dissolved TDS@ 180 C Solids, Total Suspended TSS@ 105 C Report Definitions: RL -Analyte reporting limit. QCL-Quality control limit. 419 86 0 -RL increased due to sample matrix. mgll mgll Qualifiers 0 MCLI RL OCL 10 10 Report Date: 03/12/14 Collection Date: 03/05/14 12:15 Date Received: 03/07/14 Matrix: Aqueous Method Analysis Date I By A2540 C 0311 0114 16:08 I tmm A2540 0 03111114 10:04 I alp MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of7 EN:RGY t .-q-\tJI• A10f.f l ~ '...J www.enel&)'lab.com ~ flullltlcl Slllu /til Helena, MT 877-472-0711 • Billings, MT 801·735·4489 • Casper, WY 888-235-0515 Gillette, WY 8&6-186-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 1st Quarter Surface Water 2014 Analyte Count Result Method: A2540 c Sample ID: MB·1_140310A Method Blank Solids, Total Dissolved TDS@ 180 C NO Units mg/L Sample ID: LCS-2_140310A Laboratory Control Sample Solids, Total Dissolved TDS@ 180 C 1960 mg/L Sample ID: C14030198-002A DUP Sample Duplicate Solids, Total Dissolved TDS@ 180 C 16.0 mg/L Sample ID: C14030198-003A MS Sample Matrix Spike Solids, Total Dissolved TDS@ 180 C 1130 mg/L Qualifiers: RL -Analyte reporting limit. RL %REC 7 20 98 10 11 99 Report Date: 03/12/14 Work Order: C14030228 Low Limit High Limit RPD RPDLimit Qual Batch: TDS140310A Run: BAL-19_140310A 03/10/14 16:05 Run: BAL-19_140310A 03/10/14 16:06 90 110 Run: BAL-19_140310A 03/1 0/14 16:06 3.8 5 Run: BAL-19_140310A 03/1 0/14 16:07 90 110 NO -Not detected at the reporting limit. Page 4 of7 EN:RGY t ·\hC..)f• o1·~r ... ,_._, www.energylab.com Aa/ftlell Clullfllu Sitler I BSZ Helena, MT 877-472-0711 • Billings, MT 808-735-4489 • Casper, WY 888-235-0515 Glllatte, WY 8611-&86-7175 • Rapid City, SD 888-672-1225 • College Station, 1X 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 1st Quarter Surface Water 2014 Analyte Count Result Method: A2540 D Sample ID: MB-1_140311A Method Blank Units Solids, Total Suspended TSS@ 105 C NO mg/L Sample ID: LCS-2_140311A Laboratory Control Sample Solids, Total Suspended TSS@ 105 C 100.0 mg/L Sample 10: C14030214-001A DUP Sample Duplicate Solids, Total Suspended TSS@ 105 C NO mg/L Qualifiers: RL-Analyte reporting limit. Report Date: 03/12/14 Work Order: C14030228 RL %REC Low Limit High Limit Run: BAL-19_140311A 2 Run: BAL-19_140311A 10 100 80 120 Run: BAL-19_140311A 10 NO -Not detected at the reporting limit. RPD RPDLimit Qual Batch: TSS140311 A 03/11/14 1 0:03 03/11/1410:03 03/11/14 1 0:04 5 Page 5 of? EN:RGY t ·,.,, H ."'l•:l-11. ; www.energylab.com Mll/ffbi~SIIa IISI Helena, MT 877-472-0711 • Billings, MT 801-135-4489 • Casper, WY 888-235-8515 Gillatte, WY 86&-18&-7175 • Rapid City, SD 888-172-1225 • Collage Station,TX 888-&90-2218 Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Dorian Quis Reviewed by: BL2000\khelm Reviewed Date: 3/10/2014 Shipping container/cooler in good condition? Custody seals intact on all shipping container(s)/cooler(s)? Custody seals intact on all sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.) Temp Blank received in all shipping container(s)/cooler(s)? Container/Temp Blank temperature: Water-VOA vials have zero headspace? Water-pH acceptable upon receipt? Standard Reporting Procedures: Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 2.4'C On Ice Yes O Yes 0 C14030228 Date Received: 3/7/2014 Received by: dw Carrier NDA name: No 0 No 0 No 0 No O No 0 No 0 No 0 No O No 0 No O No 0 No 0 Not Present O Not Present D Not Present 0 Not Applicable O No VOA vials submitted 0 Not Applicable 0 Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Contact and Corrective Action Comments: None Page 6 of7 Samples Shipped to: Energy Laboratories Contact: Garrin Palmer ..:::2~39~3:><S~a~lt~C~re..;.;:e~k;.;,H;.;.wy.:;...._________ Ph: 435 678 4115 Casper WY, 82601 gpalmer@energyfuels.com Chain of Custody/Sampling Analysis Request ProJect Samplers Name Sample-rs Signature 1st Quarter Surface l /~ A';:-·~ 1-=--Water2014 Garrin Palmer Time Sample ID Date Collected Collected Laboratory Analysis Requested Cottonwood Creek 315/2014 1215 Total O'lssolved Solids, Total Suspended Solids Comments: Samp!e5·are not P!eserved or filtered. RelltlQUished By:(Signature) Garri.n Pai~{J~ Date/Time Received By:(Signature) 3/6/2014 1030 Date/Time Received By:(Sfgnature) -C..l3D~ C..\4030~ Datemme Page 7ofT White Mesa Mill -Standard Operating Procedures Book #11: Environmental Protection Manual, Section 2.1 Date: 2/07 Revision: DUSA-1 Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one?.£ottonwood S£,.eekJ Westwater Canyon Other (describe). ___ _ BY: ~""'-9.....\ .... >-l.-c (.., (Sampler's initials) pH BUFFER 7.0 ___ +~· L.=-1')--pH BUFFER 4.0 __ ....:..tl.:_' u __ _ SPECIFIC CONDUCTIVITY ___ ...:..q ....!..'f...l.9 ___ ----!:u~MH~O~s STEAM DEPTH: pHofWATER _~~~-~1~7 _______ _ TEMP _...LI~g..._. Cf.!..C2.==----- • I COND umhos £$· jyl,, 3 -COND 1-1mhos l-'[(o.C( pH Units ~.00 pH units '?. 2f Temp°C /ca.er-+ Temp°C /f".ct ( COND 1-1mhos l-oz.-t COND 1-lmhos 1 '?y.;; pH units )?''' t':t-pH units 0.-z.{ Temp°C ' ~-'iter Temp°C 1?:1? Comments: b'ji)K.-J_ on '3• .k_ cA I 3 I D L, .;-r s . (•c-r c .-r. Q c.. [ l"".g c r.,.._,J ]) ru•·d T.A k """"....._ t f.u ... ,. bH'IL~ "'"'"J Co/d . LJ /"(,. 7 s....""""f'') Corle.dec-l o-f-1315. White Mesa Mill -Standard Operating Procedures Book #11: Environmental Protection Manual, Section 2.1 Date: 2/07 Revision: DUSA-1 Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one):Cottonwood Creek ~estwa er can;gyot.her (describe) ___ _ DATE:_3) I ':1/ Zol L{ BY: &&..ell', .A.. .Po.. LAA.e-C (Sampler's initials) pH BUFFER 7.0 __ 7.L...l'.__:C)=----· pH BUFFER 4.0 Ll, Q SPECIFIC CONDUCTIVITY __ _,_q--lq._9..__ ___ ~u=MH=O:::..::<s STEAM DEPTH: .AlA pHofWATER ___ ~A/~A~----------TEMP _J-_!1/X..,.,A~------- COND umbos COND w:m1os pH Units pH units Temp°C Temp °C COND J.Lmhos COND J.Lmhos pH units pH units Temp°C Temp°C Comments: 6·/6/1'1 -Ar,.l!)(.Gl. o,.._ sdc.. c..± oqoo. C,tc.et.l..)&<r by~ l~r.~ pkat-w) tl3o/it..l-Art~vc.c).. Q~ nil' l'..t-\..3JD. (rce.\C.. Wk$ tAt'( Ls'-'-pk-1-o ). l)A..~bk. "\-o ,Sc...~ l~ lou-.+~oA bc.c.&...uJ~ "'-D w"-+~ w&<-..S fr-tSe.~-L W ll\ .>t--"""-f k. c:So; Is o.. + locv-. +-. OA.. &lur;~ A ~.5u .. d· ~l.)e.v-... +. J •• . .. '. ·~ .. I EN:RGY l J\--± \-11 • •'· I ~. T 'I~ • Helena, MT 877-47Z-0711 • Billings, MT 801-735-4489 • Casper, W'f 811-235-1515 Glllatta, W'f 11&-186-7175 • Rapid City, SD 818-&72-1225 • Collage Station, TX 881-610-2211 April 29, 2014 Energy Fuels Resources (USA) Inc 225 Union Blvd Ste 600 Lakewood, CO 80228-1826 Work Order: C14040518 ANALYTICAL SUMMARY REPORT Project Name: 2nd Quarter Surface Water 2014 Energy Laboratories, Inc. Casper WY received the following 1 sample for Energy Fuels Resources (USA) Inc on 4/16/2014 for analysis. --------------------------------------------------------------------------------Lab ID Client Sample ID Collect Date Receive Date Matrix C 1404051 8-001 CottonWood Creek 04/14/14 13:15 04/16/14 Filter Test Sample Filtering Uranium, Dissolved Uranium, Suspended Digestion, Total Metals Gross Alpha, Gross Beta Radium 226, Dissolved Radium 226, Suspended Thorium, Isotopic Thorium, Suspended Isotopic Solids, Total Dissolved Solids, Total Suspended The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: 41~ c\:k )%'&___. Report Proofing Specialist Digitally signed by Kathy Hamre Date: 2014.04.29 12:48:59 -06:00 Page 1 of 12 Gilletta, WY IIB-181-7115 • Rapid City, SD 118-172-1225 • Collage Station, TX BIUID-221 8 CLIENT: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Surface Water 2014 Report Date: 04/29/14 Sample Delivery Group: C14040518 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANAL YSJS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b-Energy Laboratories, Inc. -Billings, MT eli-g-Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r-Energy Laboratories, Inc. -Rapid City, SD eli-cs-Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: US EPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001 , Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify Ell's certification coverage by visiting www.energylab.com Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 12 EN:RGY I ,"'.·tOfo"\l O I.JI. _ www.energytab.com Allll1tlal EDflla !*a llfZ Helena, MT 877 .... 72-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-1515 Gillette, WY 866-186-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Surface Water 2014 LabiD: c 1404051 8-001 Client Sample ID: CottonWood Creek Analyses PHYSICAL PROPERTIES Solids, Total Dissolved TDS@ 180 C Solids, Total Suspended TSS@ 105 C METALS-DISSOLVED Uranium METALS-SUSPENDED Uranium RADIONUCLIDES-DISSOLVED Gross Alpha Gross Alpha precision (±) Gross Alpha MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC RADIONUCLIDES-SUSPENDED Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result Units 485 mgll 12 mgll 0.0086 mgll NO mgll 13.0 pCii L 2.3 pCi!L 2.5 pCil l 0.39 pCil l 0.15 pCiiL 0.16 pCii L -0.004 pCii L 0.08 pCill 0.2 pCi!L 0.01 pCiiL 0.12 pCiiL 0.20 pCiiL 0.1 pCill 0.07 pCiiL 0.09 pCiiL MDC -Minimum detectable concentration Qualifiers D u u U -Not detected at minimum detectable concentration Report Date: 04/29/14 Collection Date: 04/14/14 13:15 Date Received: 04/16/14 Matrix: Aqueous MCL! RL QCL Method Analysis Date I By 10 A2540 C 04117114 15:21 I tmm 10 A2540 D 04118114 11 :13 I alp 0.0003 E200.8 04117114 20:49 I elm 0.0003 E200.8 04122114 21 :16 I elm E900.0 04125114 17:28 I lbb E900.0 04125114 17:28 I lbb E900.0 04125114 17:28 I lbb E903.0 04123114 06:32 I lmc E903.0 04123114 06:32 I lmc E903.0 04123114 06:32 I lmc E908.0 04123114 09:01 I dmf E908.0 04123114 09:01 I dmf E908.0 04123114 09:01 I dmf E903.0 04128114 07:48 I lmc E903.0 04128114 07:48 I lmc E903.0 04128114 07:48 I lmc E9'o8.0 04125114 08:52 I dmf E908.0 04125114 08:52 I dmf E908.0 04125114 08:52 I dmf MCL -Maximum contaminant level. NO -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 3 of 12 EI\ERGY l ~\· C.f .tol 01"1L 'j www.enefiY)eb.com Alll/tllal E"laiRw .Qallll Helena, MT 871-472-0711 • Billings, MT 801-735-4489 • Casper, WY 8811-235-1515 Gillette, WY 118-18&-7175 • Rapid City, SD 118-&72-1225 • College Station, TX 888-&90-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Surface Water 2014 Analyte Count Result Units Method: A2540 c Lab ID: MB-1_140417A Method Blank Solids, Total Dissolved TDS@ 180 C ND mg/L Lab ID: LCS-2_140417A Laboratory Control Sample Solids, Total Dissolved TDS@ 180 C 1980 mg/L Lab ID: C14040512-001 B DUP Sample Duplicate Solids, Total Dissolved TDS@ 180 C 370 mg/L Lab ID: C14040518-001A MS Sample Matrix Spike Solids, Total Dissolved TDS@ 180 C 1600 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL 7 20 10 11 Report Date: 04/29/14 Work Order: C14040518 %REC Low Limit High Limit RPD RPDLimit Qual Batch: TDS140417A Run: BAL-19_140417A 04/17/14 15:20 Run : BAL-19_14041 7A 04/17/14 15:20 99 90 110 Run : BAL-19_140417A 04/17/1415:20 0.3 5 Run: BAL-19_140417A 04/17/14 15:21 101 90 110 ND -Not detected at the reporting limit. Page 4 of 12 EN:RGY !... .. ·\J !D! -t ..... ~TC-1 .. 11 •; www.energylab.com Aalttlal Ezulaa Sl8a 111Z Helena, MT 877 .... 72-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-0515 Gillette, WY 81&-18&-7175 • Rapid City, SD BBB-&72-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Surface Water 2014 Analyte Count Result Method: A2540 D Lab ID: MBLK Method Blank Solids, Total Suspended TSS@ 105 C ND Units mg/L LabiD: LCS Laboratory Control Sample Solids, Total Suspended TSS@ 105 C 92.0 mg/L Lab ID: C14040507-002B DUP Sample Duplicate Solids, Total Suspended TSS@ 105 C 22.0 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL 2 10 10 Report Date: 04/29/14 Work Order: C14040518 %REC Low Limit High Limit RPD RPDLimit Qual Batch: TSS140418A Run: BAL-19_140418A 04/1 8/14 11 : 12 Run: BAL-19_140418A 04/18/14 11 :12 92 80 120 Run: BAL-19 140418A 04/18/14 11:13 - 4.7 5 ND -Not detected at the reporting limit. Page 5 of 12 EN:RGY l ."l.t!UftAT:.;fJII ~ www.energytab.com AltMftJal &r:e~wa .a. rw Helena, MT 877--472-0711 • Billings, MT 801-735-4488 • Casper, WY 888-235-0515 Gillette, WY 8&6-186-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Surface Water 2014 I Analyte Count Result Units RL Method: E200.8 Lab ID: ICV Initial Calibration Verification Standard Uranium 0.0507 mg/L 0.00030 Method: E200.8 Lab ID: LAB Method Blank Uranium NO mg/L 1E-05 Lab ID: LFB Laboratory Fortified Blank Uranium 0.0498 mg/L 0.00030 Lab ID: C14040511-001 AMS Sample Matrix Spike Uranium 0.0555 mg/L 0.00030 Lab ID: C14040511-001AMSD Sample Matrix Spike Duplicate Uranium 0.0564 mg/L 0.00030 Method: E200.8 Lab ID: ICV Initial Calibration Verification Standard Uranium 0.0500 mg/L 0.00030 Method: E200.8 Lab ID: MB-41163 Method Blank Uranium NO mg/L 0.0003 Lab ID: LCS2-41163 Laboratory Control Sample Uranium 0.100 mg/L 0.00030 Lab ID: C14040560-007AMS Sample Matrix Spike Uranium 0.242 mg/L 0.00030 Lab ID: C14040560-007AMSD Sample Matrix Spike Duplicate Uranium 0.242 mg/L 0.00030 Qualifiers: Report Date: 04/29/14 Work Order: C14040518 %REC Low Limit High Limit RPD RPDLimit Qual Analytical Run: ICPMS2-C_140417A 04/17/1412:35 101 90 110 Batch: R185609 Run: ICPMS2-C_140417A 04/17/1413:10 Run: ICPMS2-C_140417A 04/17/14 13:14 100 85 115 Run: ICPMS2-C 140417A 04/17/14 20:29 - 107 70 130 Run: ICPMS2-C_140417A 04/17/14 20:32 109 70 130 1.7 20 Analytical Run: ICPMS2-C_140421A 04/21 /1416:20 100 90 110 Batch: 41163 Run: ICPMS2-C_140421A 04/22/14 20:57 Run: ICPMS2-C_140421 A 04/22114 21 :00 100 85 115 Run: ICPMS2-C_140421A 04/22/14 21 :58 97 70 130 Run: ICPMS2-C_140421A 04/22/14 22:01 97 70 130 0.1 20 RL -Analyte reporting limit. NO-Not detected at the reporting limit. MDC -Minimum detectable concentration Page 6 of 12 EI\ERGY I .'\UOC.-/d•J!.tll:.:; www.energylab.com Aa/fflal ~ S111a 1SSZ Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-0515 Gillette, WY 81&-18&-7175 • Rapid Ctty, SD 888-&72-1225 • College Station, 1X 888-&90-2218 QAJQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Surface Water 2014 Analyte Method: E900.0 Lab ID: Th230-GrAB-1724 Gross Alpha Lab ID: MB-GrAB-1724 Gross Alpha Gross Alpha precision (±) Gross Alpha MDC Lab ID: C 14040086-003ADU P Gross Alpha Gross Alpha precision (±) Gross Alpha MDC Lab ID: C14040415-001 FMS Gross Alpha Lab ID: C14040415-001 FMSD Gross Alpha Count Result Units 3 3 Laboratory Control Sample 135 pCi/L Method Blank 3 pCi!L 0.8 pCi/L 1.0 pCi/L Sample Duplicate 645 27.4 11.3 pCi!L pCi!L pCi!L Sample Matrix Spike 356 pCi/L Sample Matrix Spike Duplicate 292 pCi!L Report Date: 04/29/14 Work Order: C14040518 RL %REC Low Limit High Limit Run: TENNELEC-3_140422A 115 80 120 Run: TENNELEC-3_140422A Run: TENNELEC-3_140422A Run: TENNELEC-3_140422A 84 70 130 Run: TENNELEC-3_140422A 32 70 130 RPD RPDLimit Qual 2.8 20 Batch: GrAB-1724R 04/25/14 17:27 04/25/14 17:27 04/25/14 17:28 18.5 04/25/14 17:27 04/25/14 17:27 20 s · Sample activity for this radionuclide is much larger than the spike activity added. Therefore the matrix spike recovery could not be calculated. The LCS and the RPD of the MS/MSD pair are acceptable; this batch is approved. Qualifiers: RL-Analyte reporting limit. NO -Not detected at the reporting limit. MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits. Page 7 of 12 EN:RGY ~ 1\. ~ l) f </I. t ·...:.11111 ~. www.energylab.com AlalftJAI fl&:llllla .. 11ft Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-186-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-&90-2218 QAIQC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Surface Water 2014 Analyte Count Result Units Method: Lab 10: Radium 226 E903.0 C14040518-001 OMS LabiD: C14040518-001DMSD Radium 226 Lab ID: LCS-41163 Radium 226 Lab ID: MB-41163 Radium 226 Radium 226 precision (±) Radium 226 MDC Method: E903.0 Lab ID: C14040519·001DMS Radium 226 Lab ID: C14040519-001DMSD Radium 226 Lab ID: LCS-RA226·7150 Radium 226 Sample Matrix Spike 18 pCi/L Sample Matrix Spike Duplicate 17 pCi/L Laboratory Control Sample 22.6 pCi/L 3 Method Blank ·0.02 pCi/L 0.1 0.3 pCi/L pCi/L Sample Matrix Spike 19 pCi/L Sample Matrix Spike Duplicate 20 pCi!L Laboratory Control Sample 7.8 pCi!L Report Date: 04/29/14 Work Order: C14040518 RL %REC Low Limit High Limit RPD RPDLimit Run: BERTHOLD 770-2_140422A 110 70 130 Run: BERTHOLD 770-2_140422A 104 70 130 5.8 Run: BERTHOLD 770-2_140422A 105 80 120 Run: BERTHOLD 770·2__140422A Run: G542M_140417A 84 70 130 Run: G542M_140417A 88 70 130 4.3 Run: G542M_140417A 69 80 120 Batch:41163 04/28/14 07:48 04/28/14 07:48 18.8 04/28/14 11 :15 04/28/14 11 :15 u Batch: RA226-7150 04/23/14 06:32 04/23/14 06:32 21.6 04/23/14 06:32 s · LCS response is outside of the acceptance range for this analysis. Since the MB, MS, and MSD are acceptable the batch is approved. Lab ID: MB-RA226-7150 3 Method Blank Radium 226 0.04 pCi/L Radium 226 precision (±) Radium 226 MDC Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration 0.1 0.2 U -Not detected at minimum detectable concentration pCi/L pCi/L Run : G542M_140417A ND-Not detected at the reporting limit. S -Spike recovery outside of advisory limits. 04/23/14 06:32 u Page 8 of 12 EN:RGY l t\·.~or. YIOr .. JL _; www.energylab.com Aal1tJa/ E.rallll.w Sllu IIJZ Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-1515 Gillette, WY 86&-186-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-221 B QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Surface Water 2014 Analyte Count Result Units Method: E908.0 Lab ID: LC5-RA-TH-150-2032 Thorium 230 Lab ID: C14040518-001 CM5 Thorium 230 LabiD: C14040518-001CM5D Thorium 230 LabiD: M B-RA· TH-150-2032 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Method: E908.0 Lab ID: C14040518-001 OMS Thorium 230 Lab ID: C14040518-001 DMSD Thorium 230 LabiD: LC5-41163 Thorium 230 Lab ID: MB-41163 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Qualifiers: RL -Analyte reporting limit. 3 3 MDC - Minimum detectable concentration Laboratory Control Sample 6.5 pCi/L Sample Matrix Spike 13 pCi/L Sample Matrix Spike Duplicate 13 pCi/L Method Blank 0.05 pCi/L 0.08 pCi/L 0.2 pCi/L Sample Matrix Spike 19 pCi/L Sample Matrix Spike Duplicate 17 pCi/L Laboratory Control Sample 16.4 pCi/L Method Blank 0.2 pCi/L 0.1 pCi/L 0.2 pCi/L Report Date: 04/29/14 Work Order: C14040518 RL %REC Low Limit High Limit RPD RPDLimit Qual Batch: RA-TH-IS0-2032 Run: ALPHANAL YST_140421 B 98 80 120 Run:ALPHANALYST_140421B 102 70 130 Run:ALPHANALYST_140421B 103 70 130 0.3 Run:ALPHANALYST_140421B Run:ALPHANALYST_140423A 109 70 130 Run: ALPHANAL YST _140423A 98 70 130 11 Run:ALPHANALYST_140423A 94 80 120 Run:ALPHANALYST_140423A NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration 04/23/14 09:01 04/23/14 09:01 04/23/14 09:01 44.3 04/23/14 09:01 u Batch:41163 04/25/14 08:52 04/25/14 08:52 29.9 04/25/14 08:52 04/25/14 08:52 Page 9 of 12 EN:RGY I ...,,,<.>ri"•IOI~r~:_. www.energylab.com AM/ftlal E.allllaSW. IIU Helena, MT 817--472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-1515 Gillette, WY 116-186-7175 • Rapid City, SD 188-&72-1225 • College Station,TX 888-&90-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 2nd Quarter Surface Water 2014 Ana lyle Count Result Units Method: SW6020 Lab ID: C 14040560-002ADI L Serial Dilution Uranium 3.28E-08 mg/L Lab ID: C 14040560-007 AM S Sample Matrix Spike Uranium 0.242 mg/L Lab 10: C14040560-007 AMSD Sample Matrix Spike Duplicate Uranium 0.242 mg/L Lab ID: MB-41163 Method Blank Uranium 4E-05 mg/L Lab ID: LCS2-41163 Laboratory Control Sample Uranium 0.100 mg/L Qualifiers: RL-Analyte reporting limit. MDC -Minimum detectable concentration Report Date: 04/29/14 Work Order: C14040518 RL ·%REC Low Limit High Limit RPD RPDLimit Qual Batch: 41163 Run: ICPMS2-C_140421A 04/22/14 21 :29 1.5E-10 5.3 20 Run : ICPMS2-C_140421A 04/22/14 21 :58 4.3E-05 97 75 125 Run: ICPMS2-C_140421A 04/22/14 22:01 4.3E-05 97 75 125 0.1 20 Run: ICPMS2-C 140421A 04/22/14 20:57 - 4E-05 Run: ICPMS2-C_140421 A 04/22/14 21 :00 4.3E-05 100 85 115 ND -Not detected at the reporting limit. Page 10 of 12 EI'.ERGY I '• ·• C .I~ t'> I . • ~I _. www.energylab.com Mtt/ft/al~~ IISZ Helena, MT 871-412-0111 • Billings, MT 800-735-4489 • Caspel', WY 888-235-1515 Gillette, WY 88&-686-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218 Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Debra Williams Reviewed by: BL2000\khelm Reviewed Date: 4/17/2014 Shipping container/cooler in good condition? Custody seals intact on all shipping container(s)/cooler(s)? Custody seals intact on all sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.) Temp Blank received in all shipping container(s)/cooler(s)? Container/Temp Blank temperature: Water -VOA vials have zero headspace? Water-pH acceptable upon receipt? Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes D 2.0"C On Ice Yes D Yes 0 C14040518 Date Received: 4/16/2014 Received by: dw Carrier NDA name: NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD No 0 NoD NoD Not Present D Not Present D Not Present 0 Not Applicable D No VOA vials submitted 0 Not Applicable D -----------------------------------------------------------------------------·----,- Standard Reporting Procedures: Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Contact and Corrective Action Comments: Sample will be filtered and preserved as necessary. Page 11 of 12 Sheet 1 of 1 CHAIN OF CUSTODY Samples Shipped to: ..;;;E;;;,;n~e~rg~y..:;;La;.;;,b;;;,.;o;.;.r.;;;.at;;.;;.o~rle~s;...__ ______ Contact: Garrin Palmer 2393 Salt Creek Hwy Ph: 435 678 4115 Casper WY, 82601 gpalmer@energvtuels.com Chain of Custody/Sampling Analysis Request ProJect Samplers Name Samplers Signature 2nd Quarter Surface I &~P~ Water 2014 Garrin Palmer Time SampleiD Date Collected Collected Laboratory An~is Rf!_q_uested CottonWood Creek 4/14/2014 1315 TDS TSS Dissolved Gross Alpha Su~ended U-nat Dissolved U-nat Su~ended Ra-226 Dissolved Ra-226 Su~ended Th-230 Dissolved Th.:230 Comments: Relinquished By:{Signature). Daterrime Received By:(Signature) Garrln Palmer C-;s-~ 4/14/2014 1200 Date/Time Relinquished By:(Signature) C { Lf0Lf(J5! Zf ATTACHMENT I SOIL SAMPLE GRAPHS, DATA TABLE, LABORATORY RESULTS AND QAIQC *Soil samples are collected during the third quarter. This attachment has been deliberately left blank.