DRC-2014-001903 - 0901a0688040a034

ENERGYFUELS
Energy Fuels Resources (USA) Inc
225 Union Blvd. Suite 600
Lakewood, CO, US, 80228
303 974 2140
www.energyfuels com
February 21,2014 DRC-2014-001 903
Mr. Rusty Lundberg
Director of the Utah Division of Radiation Control
State of Utah Department of Environmental Quality
195 North 1950 West
P.O. Box 144850
VIA OVERNIGHT DELIVERY
Salt Lake City, UT 84116-4850
Dear Mr. Lundberg:
Re: State of Utah Radioactive Material License No. UT1900479
White Mesa Mill, Blanding, Utah
Semi-Annual Effluent Monitoring Report for Period
July 1,2013 through December 31,2013
As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65
(subpart 1)), and License Condition 11.3A of State of Utah Radioactive Materials License No.
UT1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill
for the period July 1, 2013 through December 31, 2013.
If you have any questions regarding this report, please contact the undersigned at (303) 389-
4134.
Yours very trulyn
ENERGY FUELS RESOURCES (USA) INC.
Kathy Weinel
Quality Assurance Manager
cc: David C. Frydenlund
Harold R. Roberts
David E. Turk
Frank Filas
Jaime Massey
White Mesa Uranium Mill
Radioactive Materials License UT900479
Semi-Annual Effluent Monitoring Report
(July through December 2013)
Prepared For:
Utah Department of Environmental Quality
Division of Radiation Control
Prepared by:
Energy Fuels Resources (USA) Inc.
225 Union Boulevard, Suite 600
Lakewood, CO 80228
February 21, 2014
TABLE OF CONTENTS
1.0 INTRODUCTION .................................................................................................. 1
2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING ............... , ..................... 2
2.1 Program Overview ............................... -................................................................ 2
2.2 Sampling Protocol and Analytical Results ........................................................... 2
2.3 General Observations ......................................................................................... ..
2.4 Site Specific Sampling Data ................................................................................. 4
2.5 Radon-222 ............................................................................................................ 6
3.0 EXTERNAL RADIATION (DIRECT GAMMA) .................................................. 7
4.0 VEGETATION SAMPLES ..................................................................................... 8
5.0 STACK SAMPLING ............................................................................................... 8
6.0 SURFACE WATER MONITORING .................................................................... 11
7.0 SOIL SAMPLING ................................................................................................. 11
8.0 METEOROLOGICAL MONITORING ................................................................ 12
9.0 SIGNATURE .......................................................................................................... 13
LIST OF TABLES
Table 1 NCRP Report 94-Global Pb-210 Concentration Example
Table 2 Air Monitoring Station Results U-Nat (Comparison to Limits)
Table 3 Air Monitoring Station Results Th-230 (Comparison to Limits)
Table 4 Air Monitoring Station Results Ra-226 (Comparison to Limits)
Table 5 Air Monitoring Station Results Pb-210 (Comparison to Limits)
Table 6 Environmental OSL Dosimeter Measurements (Gamma)
Table 7 Stack Sampling Requirements
Table 8 Stack Effluent Concentrations and Release Rates
INDEX OF TABS
A High Volume Air Monitoring Stations
B BHV Air Sampling Graphs and Data Tables
Tab 1 BHV -1 Air Sampling Graphs and Data Table
Tab 2 BHV -2 Air Sampling Graphs and Data Table
Tab 3 BHV -3 Air Sampling Graphs and Data Table
Tab 4 BHV -4 Air Sampling Graphs and Data Table
Tab 5 BHV -5 Air Sampling Graphs and Data Table
Tab 6 BHV -6 Air Sampling Graphs and Data Table
C BHV Air Sampling Laboratory Results and QA/QC
D Air Particulate Loading Graphs and Supporting Data
E Environmental Gamma (OSL) Dosimeter Graphs and Supporting Data
F Vegetation Graphs, Data Table, Laboratory Results and QA/QC
G Stack Sample Laboratory Results
H Surface Water Graphs and Field Data Sheets
I Soil Sample Graphs, Data Table, Laboratory Results and QA/QC
ii
WHITE MESA URANIUM MILL
SEMI-ANNUAL EFFLUENT REPORT, JULY THROUGH DECEMBER 2013
1.0 INTRODUCTION
The White Mesa Mill (the "Mill") has established monitoring programs to evaluate
compliance with effluent limitations and to assess the potential for release of radioactive
material into the local environment. These monitoring programs were developed and
implemented at the time of Mill construction, operated with appropriate adaptation over
time, and are consistent with the Mill's State of Utah Radioactive Materials License No.
UT1900479 (the "License") and guidelines developed by the United States Nuclear
Regulatory Commission ("NRC") (NRC Regulatory Guide 4.14, Radiological Effluent
and Environmental Monitoring at Uranium Mills-Rev. 1, ML003739941), 1980).
Under these programs, the Mill monitors the following environmental media and
conditions:
a) Airborne particulate radionuclide concentrations obtained from the following
sampling stations:
• North, east and south of the Mill Site: BHV-1 and BHV-2 (north), BHV-5
(east), and BHV-4 (south). BHV-1 serves as a surrogate for the nearest
resident (BHV -1 is approximately 1.2 miles north of the Mill, but
approximately 0.4 miles closer to the Mill than the nearest resident);
• A background location distant to and west of the Mill (BHV-3) that was
monitored for airborne particulates up until November, 1995 (at which
time background was established), which is no longer monitored for air
particulates; and
• A station specifically requested by the White Mesa Ute Community south
of the Mill Site (BVH-6);
b) External (direct) gamma radiation measured at air monitoring stations BHV-1,
BHV-2, BHV-3, BHV-4, BHV-5 and BHV-6;
c) Vegetation at three site periphery locations, for uptake of radiation;
d) Stack release rates from the Mill's air emissions sources;
e) Surface water at Cottonwood Creek and, when flowing, Westwater Creek, both
located west of the Mill;
f) Soil radionuclide activity obtained near the air particulate monitoring stations,
during the third quarter of each year;
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g) Groundwater (up and down gradient) of the Mill facility; and1
h) Seeps and springs in the vicinity of the Mi11.1
This semi-annual effluent report provides the results of the specific monitoring and
sampling activities that were undertaken during the subject reporting period.
2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING
2.1 Program Overview
The environmental airborne particulate monitoring program at the Mill utilizes four air
sampling stations. Four high-volume continuous air sampling stations (BHV -1, BHV -2,
BHV -4, and BHV -5) are required by the License. These sampling stations serve as
sentinels for airborne particulate which could potentially emanate from the Mill site. In
addition to its general site monitoring function, BHV-1 also serves as a conservative
surrogate for concentrations at the nearest resident, because it is located approximately
1.2 miles north of the Mill just south of the nearest resident but between the Mill and that
resident.
With regard to background monitoring, the Mill previously operated a continuous high-
volume air sampling station (BHV-3) which was located approximately 3.5 miles west of
the Mill site. With the approval of NRC, this station (BHV -3) was removed from the
active air monitoring program in November 1995. At that time, NRC determined that a
sufficient air monitoring database had been compiled at BHV-3 to establish a
representative airborne radionuclide background for the Mill. While air sampling was
discontinued at this location, gamma measurements and soil sampling continue at BHV-
3.
In addition to the environmental air sampling locations described above, an additional
station (BHV -6) was installed at the request of the White Mesa Ute Community. This
station began operation in July of 1999 and provides airborne particulate information in
the southerly direction between the Mill and the White Mesa Ute Community.
2.2 Sampling Protocol and Analytical Results
Airborne particulate monitors are operated continuously at each of the high-volume air
sampling stations referenced above except BHV-3. Particulate sample collection filters
are gathered by site technicians weekly in accordance with the Mill's environmental air
sampling procedures and are composited on a quarterly basis for laboratory analyses.
The collected filters are analyzed for Unat activity, Th-230 activity, Ra-226 activity, and
Pb-210 activity. Fugitive dust standards for the facility are limited by the Mill's State of
Utah Air Approval Order. The specific locations of the Mill's airborne particulate
1 Groundwater sampling and seeps and springs sampling are reported separately pursuant to the Mill's State
of Utah Ground Water Discharge Permit No. UGW370004, and are not included with this report.
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monitoring stations are depicted on the figure entitled High Volume Air Monitoring
Stations included as Attachment A. Station BHV-3, which is no longer sampled for air
particulates, is located approximately 3.5 miles west of the Mill facility and is not shown
on the Figure.
The analytical results of radionuclide particulate sampling for each monitoring station
operated during this reporting period are provided in Attachment B under separate
sampling station attachment tabs (Tabs 1-6). Each tab contains graphical illustrations of
the radionuclide concentrations in log-scale presentation format. The graphs display
reported data over time since the 1981 inception of the Mill's environmental air
particulate monitoring program. The actual analytical results (and associated QA/QC
information) reported by the laboratory for the reporting period are provided under
Attachment C. In addition to the analyses for radionuclides, particulate loading is
determined for each filter and composited as a quarterly mass-loading estimate for review
purposes only. Graphs showing particulate loading at each station and the underlying data
are included as Attachment D.
The first 2 sampling periods of 2012 have been omitted from particulate loading on the
graph for BHV-6 in Attachment D. The timer on the airborne particulate monitoring
station at BHV -6 malfunctioned, and the data are considered invalid due to the inability
to measure the time sampled. The timer was replaced prior to the third sampling period in
2012 and all other measurements are valid.
For graphical il1us 'ation purpo e value reported at zero, values reported at less than
the prescribed deteetion limit < l x w -IG uCi/ml), and missing values were plotted as 1 x
10-16 uCi/ml con enttation,. Where ·other "less than" values were indicated (i.e., where
detection limits for the data varied from 1 x 10-16 uCi/ml), the detection limit
concentration was utilized for plotting the data point. This graphing convention is not
utilized to formulate station average information, nor is it intended as a precedent for data
treatment. Rather, the intent is to provide a conservative viewable depiction of site
airborne radionuclide information. This is considered to be a conservative approach,
because the actual concentration below the detection limit cannot be determined and, as a
result, the plotted point will be at the same or a higher concentration than the actual
activity concentration of the collected sample.
2.3 General Observations
The results of environmental air monitoring for this semi-annual period indicate that for
all radionuclides at all monitoring stations, airborne radionuclide particulate activity
concentrations were well below regulatory Effluent Concentration Limits ("ECL's") and
the Mill's ALARA goals, which are set at 25% of the ECLs.
It is noteworthy and expected that Pb-210 concentrations are elevated when compared to
the other parent radionuclide concentrations (i.e. U-nat, Th-230 and Ra-226). This
phenomenon is due to the well-established controlling effect experienced worldwide as a
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result of the ubiquitous presence of radon in the earth's atmosphere. Accordingly, the
elevated Pb-210 presence in disequilibrium with parent radionuclides measured here is
not associated with uranium milling operations. Rn-222 emanates as a decay-chain
progeny of the Ra-226 contained in the soil of the earth's crust and is dispersed generally
throughout the earth's atmosphere. The electrically charged short and long-lived decay
products of Rn-222 attach to ambient dust particles found naturally in the atmosphere and
are carried with the air. Pb-210 is the longest lived of these decay products and is the
decay product of the shorter-lived radon progeny. As such, it accumulates as an electrical
attachment on the natural ambient dust in the atmosphere and is generally measured at
elevated activity when compared to local decay-chain parent radionuclide activity,
regardless of uranium milling activity. At the Mill's BHV air monitoring stations, all
dust (ambient natural and mill derived) is collected by the sample filter. Because of the
natural elevation of Pb-210 accumulated as an attachment to the naturally occurring
ambient dust particles collected by the air sampling equipment, Pb-210 is commonly
elevated and in disequilibrium when compared to parent radionuclide activity, regardless
of the Mill's presence. By way of illustration, average ground-level concentrations have
been reported for selected States (NCRP Report 94, 1992) and are summarized in Table 1
below, demonstrating that elevated Pb-210 activity is present where no uranium milling
operations are located nearby. In April 1977, prior to Mill construction and Mill
operations, air f-ruti ulate Pb-210 was measured at the Mill site to be 1.3E-14 uCi/rnl
(13.0E-3 pCiJm 2•
Table 1-NCRP Report 94-Global Pb-210 Concentration Example
State Pb-210 Concentration
uBq/M" uCi/ml
California 600 1.6E-14
lllinois 1500 4.1E-14
Ohio 300 8.1E-15
Massachusetts 700 1.9E-14
2.4 Site Specific Sampling Data
The results of airborne particulate monitoring for the period (without background
subtraction) are provided by sampling station and radionuclide in Tables 2 through 5
below. Along with these data, the tables present comparative ECL's and the ECL
percentage measured at each of the monitoring stations sampled during the period. A
review of these data support the conclusion that airborne particulates are well controlled
at the Mill. In all cases, the measured activity concentrations were well within the ECL,
as well as the Mill's ALARA goal (i.e. 25% of the ECL). Lower Limits of Detection
consistent with NRC Regulatory Guide 4.14 were maintained by the Mill's contract
analytical laboratory for this reporting period.
2 See the Environmental Report, White Mesa Uranium Project, San Juan County, Utah for Energy Fuels
Nuclear, Inc. prepared by Dames & Moore, January 30, 1978, Section 2.9.1.1
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The data obtained since program inception in 1981 indicates that only one individual
quarterly measurement (Th-230 at BHV-5 for the 2"d Quarter of 1996) has ever exceeded
the ECL at the Mill. While it is important to consider and evaluate an individual
measurement exceeding the ECL, it is the average annual concentration 'that is of primary
significance for public dose estimation purposes. In that instance, the average annual
concentration of Th-230 for BHV-5 in 1996 was well below the ECL. Data obtained
since program inception in 1981 also indicate that, with very few exceptions, the gross
(background inclusive) measurements do not exceed the site's ALARA goal (i.e. only
nine of the several thousand total gross radionuclide determinations to date exceeded the
Mill's self-imposed 25% ALARA goal).
Table 2-Air Monitoring Station Results U-Nat (Comparison to Limits) 3rd and 4th
Quarters 2013
Monitoring 3rd Qtr. 4th Qtr. Effluent Average
Station Result Result Concentration Percent
(uCilml) (uCilml) Limit (ECL) ECL
(uCi/ml)
BHV1 8.89E-16 5.21E-16 9.00E-14 7.83E-01
BHV2 1.76E-16 6.20E-16 9.00E-14 4.42E-01
BHV4 2.98E-15 3.88E-15 9.00E-14 3.81E+00
BHV5 2.78E-15 6.70E-15 9.00E-14 5.27E+00
BHV6 2.68E-15 1.60E-14 9.00E-14 1.04E+01
Table 3-Air Monitoring Station Results Th-230 (Comparison to Limits) 3rd and 4th
Quarters 2013
Monitoring 3rd Qtr. 4th Qtr. Effluent Average
I Station Result Result Concentration Percent
(uCilml) (uCilml) Limit (ECL) ECL
= (uCilml)
BHVl 9.13E-17 4.34E-17 2.00E-14 3.37E-01
BHV2 2.52E-17 4.19E-17 2.00E-14 1.68E-01
BHV4 4.49E-16 1.03E-16 2.00E-14 1.38E+00
BHV5 6.92E-16 3.93E-16 2.00E-14 2.71E+00
BHV6 3.97E-16 2.48E-16 2.00E-14 1.61E+00
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Table 4-Air Monitoring Station Results Ra-226 (Comparison to Limits) 3rd and 4th
Quarters 2013
Monitoring 3rd Qtr. 4th Qtr. Effluent Average
Station Result Result Concentration Percent
(uCilml) (uCilml) Limit (ECL) ECL
(uCi/ml)
BHV1 1.05E-16 3.70E-17 9.00E-13 7.89E-03
BHV2 6.13E-17 3.72E-17 9.00E-13 5.47E-03
BHV4 1.54E-16 4.47E-17 9.00E-13 1.10E-02
BHV5 3.29E-16 2.53E-16 9.00E-13 3.23E-02
BHV6 1.04E-16 1.05E-16 9.00E-13 1.16E-02
Table 5-Air Monitoring Station Results Pb-210 (Comparison to Limits) 3rd and 4th
Quarters 2013
Monitoring 3rd Qtr. 4th Qtr.
I
Effluent Average I
Station Result Result Concentration Percent
(uCilml) (uCi/ml) Limit (ECL) ECL
(uCilml)
BHVl 8.00E-15 2.59E-14 6.00E-13 2.83E+00
BHV2 4.90E-15 2.50E-14 6.00E-13 2.49E+00
BHV4 7.49E-15 2.93E-14 6.00E-13 3.07E+00
BHV5 6.62E-15 2.78E-14 6.00E-13 2.87E+00
BHV6 6.13E-15 2.67E-14 6.00E-13 2.74E+00
2.5 Radon-222
Due to the unavailability of monitoring equipment to detect the revised 10 CPR Part 20
standard, and with the approval of the NRC, Radon 222 monitoring at BHV stations was
discontinued in 1995. Instead, compliance with these limits and the requirements of
R313-15-301 is demonstrated by a calculation, authorized by the NRC and as
contemplated by R313-15-302(2)(a). A copy of the Technical Evaluation Report
evidencing such approval was enclosed with correspondence to the Division of Radiation
Control ("DRC") on July 28, 2008.
This calculation is performed by use of the MILDOS code for estimating environmental
radiation doses for uranium recovery operations (Strenge and Bender 1981) and more
recently in 2003 by use of the updated MILDOS AREA code (Argonne 1998). The
analysis under both the MILDOS and MILDOS AREA codes assumes the Mill to be
processing high grade Arizona Strip ores at full capacity, and calculates the
concentrations of radioactive dust and radon at individual receptor locations around the
Mill.
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The MILDOS and MILDOS AREA codes calculate the combined Total Effective Dose
Equivalent ("TEDE") from all relevant pathways, including both air particulate and
radon, at a number of locations including the nearest residence (the individual likely to
receive the highest dose from the licensed operation), approximately 1.6 miles north of
the Mill. These calculations reveal projected doses to the individual likely to receive the
highest dose from the licensed operations to be well below the 100 mrem regulatory limit
in R313-15-301(1)(a) for all pathways, including air particulate and radon, and well
below the ALARA goal of 10 mrernlyr for air emissions excluding radon as set out in
R313-15-101(4). MILDOS AREA modeling was recently conducted in support of the
Mill's 2007 License Renewal Application, utilizing the MILDOS-AREA code (Version
2.20B), to estimate the dose commitments at various receptor locations for processing of
Colorado Plateau ore (0.25% U30s and 1.5% V20 5) and Arizona Strip ore (0.637%
U30 8). The process rate was assumed to be at full capacity of 730,000 tons per year (an
average of 2,000 tons per day) with an average uranium recovery yield of 94%. That
modeling showed a TEDE of 2 mrem per year at the nearest resident (3 mrem per year at
the nearest potential residence, being the location of BHV -1 at the northern property
boundary of the Mill site), which included the dose from all radionuclide sources,
including radon. The modeled dose from radon itself was therefore a fraction of the
TEDE and well within the regulatory limits.
3.0 EXTERNAL RADIATION (DIRECT GAMMA)
Gamma exposure rate estimates were measured for the reporting period utilizing optically
stimulated luminescence dosimeters ("OSLs"). These dosimeters were located at each of
the Mill's high-volume air sampling stations (BHV-1, BHV-2, BHV-4, BHV-5 and
BHV-6) and at the designated background monitoring station (BHV-3). Measurements
obtained from location BHV-3 have been designated as background due to BHV-3's
remoteness from the Mill site (i.e., BHV-3 is located approximately 3.5 miles west of the
Mill site). The results of the environmental OSL measurements and semi-annual
cumulative above-background data are provided in Table 6 below. In addition,
measurement data obtained at these locations are graphically presented in Attachment E
to this report.
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Table 6-Environmental Optically Stimulated Luminescence Dosimeter
~easurements ((;amma)
Monitoring 3rd Qtr [ 4th Qtr IIi 3rd Qtr 4th Qtr Cumulative
Station Result Result Result Less Result Less Semi-
(mrem) (mrem) Background Background Annual
(mrem) (mrem) Estimate
(mrem)
BHV1 33.5 38.9 3.9 7.5 11.4
BHV2 31.5 33.3 1.9 1.9 3.8
BHV3 29.6 31.4 0.0 0.0 0.0
BHV4 34.5 32.1 4.9 0.7 5.6
BHV5 34.6 38.0 5.0 6.6 11.6
BHV6 30.4 33.7 0.8 2.3 3.1
The results for this period indicate that above background measurements for stations
BHV-1, BHV-2, BHV-4, BHV-5 and BHV-6 are within regulatory limits. BHV-1 is at
the location of the nearest potential residence. The nearest actual residence is
approximately 0.4 miles north of BHV-1. The annual limit for an individual member of
the public is 100 mrem/yr for combined internal and external exposure.
4.0 VE(;ETATION SA~PLES
Vegetation samples are collected at three locations around the Mill property. The
sampling locations are: 1) northeast, 2) northwest and 3) southwest of the Mill facility.
The NRC Regulatory Guide 4.14 requires that three samples be collected during the
grazing season, without specifying exact months or times during the season. During the
2013 grazing season, three sets of samples were collected on April 30, 2013, June 20,
2013, and November 14, 2013. The data from the April and June sampling events were
included in the January through June 2013 Semi-Annual Effluent Report ("SAER")
which was submitted to the DRC on August 29, 2013. Data from the November sampling
event is included in this report.
Graphical log-scale presentation of the vegetation sampling results, together with the
analytical results reported by the Mill's contract laboratory (including QA/QC
information) for this sampling period, are included as Attachment F of this report. The
2013 data results are within the variation of previous sampling episodes.
5.0 STACK SAMPLIN(;
Under Section 5.0 of Tab 1.4 of the Mill's Environmental Protection Manual, Revision:
EFR-3, 12112 (the "Environmental Protection Manual") gas stack samples are collected
at the Mill in accordance with the calendar year schedule shown below:
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Table 7 -Stack Sampling Requirements
Frequency Feed Stack (Grizzly Stack for Packaging
Baghouse) Yellowcake Dryer (Yellowcake
Bag_house)
Quarterly None If operating, U-nat If operating, U-nat
Semi-annually If operating, U-nat, If operating, U-nat, If operating, U-nat,
Th-230 Th-230, Ra-226, Pb-Th-230, Ra-226,
210 Pb-210
The analytical results of stack sampling conducted for the 3rd and 4th quarters of 2013, as
well as for the 1st and 2nd quarter of 2013, are provided in Table 8 below, indicating the
uCi/cc concentration in the stack emissions and the stack's radionuclide release rate
(uCi/sec) for U-Nat, Th-230, Ra-226 and Pb-210 at each of the stacks sampled. The
actual analytical results reported by the laboratory for the 3rd and 4th quarters of 2013 are
provided in Attachment G to this report.
As shown on Table 8, due to operational conditions at the Mill during the 1st quarter of
2013, EFRI was unable to achieve the steady state required for representative stack
sampling at the yellowcake dryers and the yellowcake baghouse as required by NRC
Regulatory Guide 4.14. The Mill did not operate during January 2013. The grizzly
baghouse operated periodically during February and March 2013. The south yellowcake
dryer and yellowcake packaging baghouse operated only intermittently during February
and March 2013 due to multiple dryer equipment shutdowns. As a result of the repeated
startups and shutdowns, the dryers only achieved representative steady state conditions,
suitable for stack monitoring during the 1st quarter of 2013. The south yellowcake dryer,
yellowcake baghouse, and the grizzly baghouse operated at a steady state in the 2nd
quarter of 2013 and were sampled as required.
The south yellowcake dryer and yellowcake baghouse operated during the 3rd and 4th
quarters of 2013. The north yellowcake dryer has not been in operation since the 3rd
quarter of 2012, and therefore, has not been sampled since it was last in operation. The
grizzly baghouse did not operate during the 3rd or 4th quarters of 2013, and therefore, was
not sampled during this reporting period.
It is also important to note that stack effluent concentrations are not comparable to
environmental air sampling station ECL' s for regulatory compliance purposes. The ECL
is a limit that applies to the receptor locations and is not applicable to effluents from mill
processes on the Mill site. These stack release data are more appropriately utilized for
dose modeling purposes, and dose modeling is not computed for semi-annual reporting
purposes.
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Table 8-Stack Effluent Concentrations and Release Rates
U-Nat U-Nat. Th-230 Th-230 Ra-226 Ra-226 Pb-210 Pb-210
u/Ci/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec
1st Qtr. 2013*
South YC Not Not Not Not Not Not
Dryer, Run 1 EFRI was unable to Required Required Required Required Required Required
South YC sample in the 1st quarter Not Not Not Not Not Not of 2013 due to Dryer, Run 2 operational conditions Required Required Required Required Required -Required
Yellowcake at the Mill. Not Not Not Not Not Not
Baghouse Required Required Required Required Required Required
2nd Qtr, 2013*
South YC
Dryer, Run I 2.94E-09 2.6IE-03 8.51E-I4 7.55E-08 1.07E-I4 9.52E-09 3.59E-13 3.I9E-07
South YC
Dryer, Run 2 2.86E-09 2.56E-03 8.75E-I4 7.85E-08 5.54E-I4 4.96E-08 3.95E-13 3.54E-07
Yellowcake
Baghouse 3.93E-08 6.29E-02 5.04E-12 8.07E-06 1.20E-13 1.92E-07 5.98E-13 9.58E-07
Grizzly Not Not Not Not
Baghouse 1.68E-1 1 l.llE-05 1.80E-13 1.18E-07 Required Required Required Required
3rd Qtr 2013*
South YC Not Not Not Not Not Not
Dryer, Run 1 3.89E-10 2.50E-04 Required Required Required Required Required Required
South YC Not Not Not Not Not Not
Dryer, Run 2 2.30E-07 1.34E-01 Required Required Required Required Required Required
Yellowcake Not Not Not Not Not Not
Baghouse 1.04E-08 1.73E-02 Required Required 1 Required Required Required Required
4th Qtr. 2013*
South YC
Dryer, Run I 2.70E-10 1.66E-04 2.33E-14 1.43E-08 7.77E-I5 4.76E-09 2.11E-13 1.29E-07
South YC
Dryer, Run 2 2.66E-IO 1.65E-04 1.48E-13 9.13E-08 2.35E-I4 I.46E-08 1.65E-13 1.02E-07
Yellowcake
Baghouse 8.91E-09 l.SSE-02 1.67E-11 2.9IE-05 4.60E-13 8.01E-07 1.16E-I2 2.03E-06
Grizzly Not in Not in Not in Not in Not Not I Not Not
Baghouse** operation operation operation operation Required Required Required Required
*The North Yellowcake Dryer was not in operation during 2013.
**The Grizzly Baghouse was not in operations during the 3'u and 41h quarters of 2013.
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6.0 SURFACE WATER MONITORING
Under the License, Part 11.2 B surface water samples are required to be obtained
annually from Westwater Canyon and semi-annually from Cottonwood Creek. Sediment
samples from Westwater Canyon are taken in place of the Westwater Canyon surface
water sample where surface water is not available for sampling.
Westwater Canyon surface water was not sampled in the first or second quarter of 2013,
because no water was present during the reporting period. A surface water sample was
collected from Westwater Canyon in the third quarter of 2013, and was analyzed for the
constituents required by the License, Part 11.2 B. As shown on the labonitory data report
in Attachment H, the total dissolved solids ("TDS") result for Westwater Canyon is "H"
flagged, indicating the analysis was completed outside of the recommended method
holding time. The laboratory noted that the TDS result was analyzed past the
recommended holding time due to reanalysis required due to severe matrix interference.
The original analysis was completed on September 13, 2013 within holding time,
however, sample matrix interference caused the result to be non-detect at an increased
reporting limit. The sample was reanalyzed six more times in an effort to achieve a result
above the reporting limit. The matrix interference was most likely caused by the
significant amount of rainfall seen at the Mill during September 2013. The rainfall made
it possible to collect a sample from the Westwater Canyon, however; the increased water
flow caused the sample to have a high solids content which caused the matrix
interference. When a reportable result was achieved by the laboratory, the holding time
had already expired. These data are considered useable for the intended purposed,
because there are duplicate analyses to support the reported result.
The Mill's Environmental Protection Manual requires that samples from Cottonwood
Creek be analyzed for TDS and total suspended solids ("TSS") quarterly, and the
License, Part 11.2 B requires that samples from Cottonwood Creek be analyzed for
dissolved and suspended radionuclides including Gross Alpha, U-nat, Ra-226, and Th-
230 emi -annually. In accordance with these requirements, Cottonwood Creek was
ampled for TDS and TSS during the 3rd quarter, and was sampled for TDS, TSS, and the
radionuclide: durii:tg th 4th quarter.
The field data sheets for the surface water sampling events, along with graphs showing
historic results are included as Attachment H. The results of this sampling indicate that
surface water concentrations remain low and within the range of typical background
levels.
7.0 SOIL SAMPLING
Under Tab 4.1 of the Mill's Environmental Protection Manual, surface soils are required
to be sampled at the Mill's air monitoring stations (BHV-1, BHV-2, BHV-3, BHV-4,
BHV -5 and BHV -6) once per year during August or as soon as possible thereafter, but no
later than September 30 of each year. In accordance with the Mill's Environmental
11
N:\WMM\Required Reports\Semi Annual Effluent Reports\2013 July-Dec\July_Dec 2013_SAER_text.docx
Protection Manual, surface soils were collected in August 2013. The soil samples were
analyzed, on a dry basis, for Ra-226 and U-nat. The results of these samplings indicate
that soil activity levels at the air monitoring stations remain low and within the range of
typical background levels. A graphical presentation of the historical results for soils at the
air monitoring stations, together with analytical sample results for the August 2013
sampling are provided in Attachment I.
8.0 METEOROLOGICAL MONITORING
As in prior reporting periods, an independent contractor has prepared the White Mesa
Mill Semi-annual Meteorological Monitoring Report for the period of July through
December 2013. This information is retained at the Mill site for agency review.
12
N:\WMM\Required Reports\Semi Annual Effluent Reports\2013 July-Dec\July_Dec 2013_SAER_text.docx
9.0 SIGNATURE
This report was prepared by Energy Fuels Resources (USA) Inc. on February 21, 2014
Energy Fuels Resources (USA) Inc.
Frank Filas
Vice President, Permitting and Environmental Affairs
13
N:\WMM\Required Reports\Semi Annual Effluent Reports\2013 July-Dec\July_Dec 2013_SAER_text.docx
ATTACHMENT A ·
HIGH VOLUME AIR MONITORING STATIONS
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0 Air Monitor
Stations
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'· ~ -._,:\_ ,1 = I ./... f ~~,, : -o ____ j _______ _ .:,, ~~----j---o 6 -----------\.\~ .. ,. ~ '~
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Eaergy hek Resources (USA) lac.
WHITE MESA Mill.
ATTACHMENT B
BHV AIR SAMPLING GRAPHS AND DATA TABLES
TAB 1
BHV-1 AIR SAMPLING GRAPHS AND DATA TABLE
Date Effluent Concentration limit= 9E-14 uCi/ml BHV-1U ~ffluent Concentration Limit = 2E-14 uCi/ml BHV-lT Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit= GE-13 uCifml BHV-1PB'
ALARAGoal = 2.25E-14 uCi/ml /ILARAGoal = SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml
Pre 1994 MPC limit = SE-12 uCi/ml Pre 1994 MPC limit"' BE-14 uCi/ ml Pr:al!J94 MI'C limit." ZE-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml
Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = "IE-12 uCi/ml
Cone EFC EFCA Cone fFC EFCA Cone EFC EFCA Cone EFC EFCA
9/28/1981 2.35E-15 S.OOE-12 1.25E-12 7.82E-16 B.OOE-14 2.00E-14 1.06E-15 2.00E-12 5.00E-13 2,57E-14 4.00E-12 l.OOE-12
12/14/1981 1.56E-15 5.00E-12 1.25E-12 1.49E-15 8.00E-14 2.00E-14 1.93E-15 2.00E-12 5.00E-13 2.64E-14 4.00E-12 l.OOE-12
3/29/1982 2.16E-15 5.00E-12 1.25E-12 2.93E-15 8.00E-14 2,00E-14 1.16E-15 2.00E-12 5.00E-13 2.09E-14 4.00E-12 l.OOE-12 !
6/30/1982 4.69E-15 ·5.00E-12 1.25E-12 3.46E-15 8.00E-14 2.00E-14 2.38E-15 2.00E-12 5.00E-13 2.14E-14 4.00E-12 l.OOE-12
9/27}1982 4.45E-15 5.00E-12 1.25E-12 3,29E-15 8.00E-14 2.00E-14 3.23E-15 2.00E-12 5.00E-13 1.99E-14 4.00E-12 l.OOE-12 ,
1/3/1983 4.39E-15 5.00E-12 1.25E-12 5.91E-16 8.00E-14 2.00E-14 9.14E-16 2.00E-12 5.00E-13 4.87E-14 4.00E-12 l.OOE-12
4/4/1983 7.51E-16 5.00E-12 1.25E-12 2.13E-16 8.00E-14 2.00E-14 3.20E-16 2.00E-12 5.00E-13 1.88E-14 4.00E-12 l.OOE-12 i
6/30/1983 2,68E-16 5.00E-12 1.25E-12 6.92E-16 8.00E-14 2.00E-14 7.92E-16 2.00E-12 S.OOE-13 2.00E-14 4.00E-12 l.OOE-12 I
10/3/1983 5.00E-12 1.25E-12 8.00E-14 2.00E-14 O.OOE+OO Z.OOE-12 !i.OOE-13 4.00E-12 1.00E-12
1/3/1984 2.87E-15 5.00E-12 1.25E-12 1.14E-16 8.00E-14 2.00E-14 1.79E-16 2.00E-12 !;.OOE-13 1.06E-14 4.00E-12 l.OOE-12
412/1984 1.59E-15 5.00E-12 1.25E-12 3.40E-16 8.00E-14 Z.OOE-14 3.71E-16 z.OOE-12 s.OOE-13 3.34E-14 4.00E-12 1.00E-12
7/2/1984 3.10E-15 5.00E-12 1.25E-12 1.00E-15 8.00E-14 2.00E-14 2.09E-15 2.00E-12 5.00E·13 1.88E·14 4.00E-12 1.00E-12
10/1/1984 6.42E-16 5.00E-12 1.25E-12 1.39E-16 8.00E-14 2.00E-14 1.94E-16 Z.OOE-12 5.00E-13 1.85E-14 4.00E-12 l.OOE-12
1/2/1985 5.06E-16 5.00E-12 1.25E-12 4.56E-16 8.00E-14 Z.OOE-14 3.49E-16 Z.OOE-12 5.00E-13 3.03E-14 4.00E-12 l.OOE-12
4/1/1985 O.OOE+OO 5.00E-12 1.25E-12 1.23E-15 8.00E-14 Z.OOE-14 4.88E-16 2.00E-12 S.OOE-13 8.06E-15 4.00E-12 l.OOE-12
7/1/1985 7.17E-16 5.00E-12 1.25E-12 8.00E-14 2.00E-14 1.05E-15 Z.OOE-12 S.OOE-13 2.15E-14 4.00E-12 l.OOE-12
9/30/1985 6.13E-16 5.00E-12 1.25E-12 1.18E-16 8.00E-14 Z.OOE-14 3.71E-16 Z.OOE-12 5.00E-13 3.64E-15 4.00E-12 l.OOE-12
1/2/1986 3.42E-15 5,00E-12 1.25E-12 4.74E-16 8.00E-14 Z.OOE-14 Z.OOE-12 S.OOE-13 4.00E-12 l.OOE-12
4/1/1986 3.98E-15 5,00E-12 1.25E-12 9.74E-16 B.OOE-14 Z.OOE-14 1.50E-15 Z.OOE-12 S.OOE-13 1.41E-14 4.00E-12 1,00E-12
6/3()/1.986 5.51E-17 5.00E-12 1.25E-12 3,52E-16 8.00E-14 2.00E-14 1.37E-15 2.00E-12 5.00E-13 1.23E-14 4.00E-12 1.00E-12
10/27/1986 1.99E-15 5.00E-12 1.25E-12 ,3.06E-16 8.00E-14 2.00E-14 1.25E-15 2.00E-12 5.00E-13 1.08E-14 4.00E-12 1.00E-12
12/15/1986 1.67E·15 5.00E-12 1.25E-12 1.16E-16 8.00E-14 2.00E-14 5,98E-16 2.00E-12 5.00E-13 1.37E-14 4.00E-12 l.OOE-12
3/16/1987 2.33E-15 5.00E-12 1.25E-12 4.30E-16 i!.OOE-14 2.00E-14 1.92E-16 2.00E-12 5.00E-13 5.59E-14 4.00E-12 l.OOE-12
5/11/1987 2.36E-15 5.00E-12 1.25E-12 7.69E-16 8.00E-14 2.00E-14 8.76E-16 2,00E-12 5.00E-13 1.45E-14 4.00E-12 1.00E-12
9/9/1987 2.27E-15 5.00E-12 1.25E-12 2.44E-15 S.OOE-14 2.00E-14 8.51E-16 2.00E-12 5.00E-13 3.14E-14 4.00E-12 1.00E-12
11/2/1987 2.75E-15 S.OOE-12 1.25E-12 2.46E-15 B.OOE-14 2.00E-14 1.34E-15 Z.OOE-12 5,00E-13 2.79E-14 4.00E-12 1.00E-12 1
2/16/1988 1.07E-15 5.00E-12 1.25E-12 1.47E-16 8.00E-14 2.00E-14 4.44E-16 2.00E-12 5.00E-13 4.01E-14 4.00E-12 l.OOE-12
5/18/1988 1.98E-15 S.OOE-12 1.25E·12 1.25E-15 B.OOE-14 2.00E-14 6.40E-16 2.00E-12 5.00E-13 1,07E-14 4.00E-12 l.OOE-12
8/15/1988 2.06E-15 5.00E-12 1.25E·12 3.41E-15 B.OOE-14 2.00E-14 5.08E-16 2.00E-12 5.00E-13 1.62E-14 4.00E-12 l.OOE-12
11/14/1988 3.94E-15 S.OOE-12 1.25E-12 2.12E-15 8.00E-14 2.00E-14 1,01E-15 2.00E-12 5.00E-13 2.47E-14 4.00E-12 l.OOE-12
2/13/1989 1.99E-15 5.00E-12 1.25E-12 5.73E-16 S.OOE-14 2.00E-14 5.99E-16 2.00E-12 5.00E-13 3.23E-14 4.00E-12 l.OOE-12
5/15/1989 1.70E-15 S.OOE-12 l.25E-12 6.32E-16 8.00E-14 2.00E-14 5.86E-16 2.00E-12 5.00E-13 6.16E-15 4.00E-12 l.OOE-12
8/14/1989 2.31E-15 5.00E-12 1.25E-12 2.31E-16 8.00E-14 2.00E-14 1.77E-16 2.00E-12 5.00E-13 7.65E-15 4.00E-12 l.OOE-12
11/13/1989 4.72E-15 S.OOE-12 1.25E-12 1.71E-15 B.OOE-14 2.00E-14 1.52E-15 2.00E-12 5.00E-13 1.89E-14 4,00E-12 !.OOE-12
2/12/1990 3.44E-16 S.OOE-12 1.25E-12 8.39E-16 8.00E-14 2,00E-14 8.31E-16 2.00E-12 5.00E-13 2.57E-14 4,00E-12 1,00E-12
5/14/1990 3.03E-15 5.00E-12 1.25E-12 1.47E-15 8.00E-14 2.00E-14 1.04E-15 2.00E-12 5.00E-13 1.79E-14 4..00E-12 1,00E-12
8/13/1990 1.64E-15 5.00E-12 1.25E-12 1.49E-15 8.00E-14 2.00E-14 3.34E-16 2.00E-12 5.00E-13 8.27E-15 4.00E-12 l.OOE-12
11/12/1990 1.48E-15 S.OOE-12 1.25E-12 7.50E-16 8.00E-14 2.00E-14 5.80E-16 2.00E-12 5.00E-13 2.16E-14 4.00E-12 l.OOE-12
2/11/1991 1.90E-16 S.OOE-12 1.25E-12 3.48E-17 8.00E-14 2.00E-14 7.91E-17 2.00E-12 S.OOE-13 3.79E-14 4.00E-12 1.00E-12
5/13}1991 3.42E-16 S.OOE-12 1.25E-12 1.34E-15 B.OOE-14 2.00E-14 7.39E-16 2.00E-12 5.00E-13 1.46E-14 4.00E-12 l.OOE-12
8/12/1991 2.77E-16 S.OOE-12 1.25E-12 4.17E-17 B.OOE-14 2.00E-14 l.45E-16 2.00E-12 5.00E-13 1.80E-14 4.00E-12 l.OOE-12
11/11/1991 6.65E-17 S.OOE-12 1.25E-12 9.13E-17 8.00E-14 2.00E-14 2.77E-17 2.00E-12 5.00E-13 l.OGE-14 4.00E-12 l.OOE-12
2/10/1992 1.94E-16 S.OOE-12 1.25E-12 4.28E-17 8,00E-14 2.00E-14 4.08E-17 2.00E-12 5.00E-13 3.51E-14 4.00E-12 l.OOE-12
5/11/1992 .2.54E·16 5.00E-12 1.25E-12 6.49E-16 8.00E-14 2.00E-14 p.86E-17 Z.OOE-12 S.OOE-13 l.38E-14 4.00E-12 l.OOE-12
8/10/1992 1.73E-16 5.00E-12 1.25E-12 1.55E-16 8.00E-14 2.00E-14 l.20E-16 2.00E-12 S.OOE-13 1.53E-14 4.00E-12 1.00E-12
11/9/1992 1.56E-16 5.00E-12 1.25E-12 3,19E-17 8.00E-14 Z.OOE-14 4.90E-18 Z.OOE-12 5.00E-13 l.86E-14 4.00E-12 l.OOE-12
2/9/1993 ,2.10E-16 5.00E-12 1.25E-12 8.00E-14 Z.OOE-14 3.89E-17 z.OOE-12 5.00E-13 2.52E-14 4.00E-12 l.OOE-12
5/10/1993 l.OOE-16 5.00E-12 1.25E-12 4.11E-17 8.00E-14 ;>..OOE-14 6.43E-17 Z.OOE-12 5.00E-13 1.26E-14 4.00E-12 l.OOE-12
8/10/1993 '2.30E-16 5.00E-12 1.25E-12 G.OOE-17 B.OOE-14 2.00E-14 6.43E-17 2.00E-12 S.OOE-13 1.60E-14 4.00E-12 l.OOE-12
11/8/1993 S.OOE-12 1.25E-12 B,OOE-14 Z.OOE-14 O.OOE+OO Z.OOE-12 5.00E-13 1.57E-14 4.00E-12 l.OOE-12
2j7j1994 1.82E-16 5.00E-12 1.25E-12 5.00E-18 B.OOE-14 2.00E-14 4.30E-17 Z.OOE-12 s.OOE-13 2.59E-14 4.00E-12 l.OOE-12
5/9/1994 3.60E-16 5.00E-12 1.25E-12 2.70E-16 S.OOE-14 ;>..OOE-14 2.87E-16 Z.OOE-12 S.OOE-13 l.GOE-14 4.00E-12 1.00E-12
8/9/1994 4.04E-16 5.00E-12 1.25E-12 2.70E-16 8.00E-14 2.00E-14 2,94E-16 2.00E-12 5.00E-13 2.00E-15 4.00E-12 l.OOE-12
1117}_!994 9.18E-17 5.00E-12 1.25E-12 3.60E-16 --8.00E-14 2.00E-14 2,91E-16 2.00E-12 (5.00E-13 2.00E-15 4.00E-12 l.OOE-12
Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-1U EfRuent Concentration Limit= ZE-14 uCi/ml BHV-1T Effluent Concentration Limit= 9E-13 uCl/ml BHV-1R Effluent Concentration Limit= !.E-13 uCi/ml BHV-1PB
ALARAGoal= 2.25E-14 uCi/ml ALARA·Goal = SE-13 uCi/ml ALARAGoal= 2.25E·13 UCI/ml ALARAGoal = 1.5E-13 uCi/ml
Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC Limit= BE-14 uCi/ml Pre 1994 MPC Limit= 2E-12 uCi/ml Pre 1994 MPC Limit= 4£-12 uCl/ml
Pre 1994 ALARA GOAL= t:m-12 uCi/ml Pre 1994 ALARA GOAL= 5E-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 u:Ofm I
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
2/7/1995 1.77E-15 9.00E-14 2.25E-14 9.70E-17 l .OOE-14 S.OOE-15 9.70E-17 9.00E-13 2.25E-13 8.60E-15 6.00E-13 1.50E-13
5/9l1995 9,40E·l7' 9.00E-14 2.25E-14 5.36E·l& l .OOE-14 S,OOE-15 1.60E-15 9.00E-13 2.25E-13 3.84E-15 6.00E-13 1.50E-13
'Q/:9/1995 2.70E"l5 9.00E-14 l.25E-14 1.60E-16 2.00E-14 S.OOE-15 2.76E-16 9.00E-13 2.25E-13 3.76E-15 6.00E-13 l.SOE-13
ll/ll/~95 4.SUE-1S 9.00E·l!l 2.25E-14 6.41E-16 2.00E-14 5.00E-15 8.93E-16 9.00E-13 2.25E-13 5.20E-15 6.00E-13 l.SQf.-.U
2/S/l99fi 5.34E-15 g.OOE-14 2.25E-14 2.30o·lS l .OOE-14 5.00E-15 1.30E-15 9.00E-13 2.25E-13 4.20E-15 6.00£..13 1.50£-13
S/~/1996 S.llE-16 9.00E-14 1.25E-14 3:06!:·16 l.OOE-14 5.00E-15 1.40E-16 9.00E-13 2.25E-13 7.03E-15 6.00E-13 l.SOE-.13
S/5/l995 5,99!:-:;t6 9,00E-14 t2SE·14 1.55E-15 l.OOE-14 5.00E-15 2.03E-16 9.00E-13 2.25E-13 5.94E-15 6.00E-13 1.50E-13
U/6/1996 3.3&f.-.16 9.00E·14 2.25E-14 5.45E-16 Z.OOE-14 S.OOE-15 l.OOE-16 f9.0DE-13 2.25E-13 1.22E-14 6,00E-13 1.50E-13
2/6/1997 .ux\t,t6 9.00E-14 2.25E-14 1.25E-16 2.00E-14 5.00E-15 1.28E-16 9.00E-13 Z.25E-13 5.68E-15 6.00E-13 1.50E-13
5/5jl!J97 1.09E-16 9.00E-14 2.25E-14 1.00E-16 Z.OOE-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 4.39E-15 6.00E-13 1.50E-13
8/l.l/l!J'J7 2.88&16 9.00E-14 2.25E-14 3.83E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 5.29E-15 G.OOE,l3 l.SOE-13
[/5/19'18 3.2410-16 9.00E-14 2.25E-14 3.47E-16 l .OOE-14 S.OOE-15 1.19E-16 9.00E·13 2.25E-13 4.73E-15 6.00E-13 1.50E-13
4/28/1998 4.75E-i6 9.00E-14 '2.25E-14 6.73E-16 2.00E-14 5.00E-15 5.69E-16 9.00E-13 2.25E-13 5.94E-15 6.00E-13 1,50E-13
7/31/1998 8.84E'·lii 9.00E-14 2.25E-14 l,93E-15 2.00E-14 5.00E-15 1A3E-15 9.00E-13 2.25E-13 5.22E-15 6.00E-13 1.50E-13
9/28/1998: 2.81E-16 9.00E-14 2.25E-14 2.89E-16 2.00E-14 5.00E-15 1.80E-16 9.00E-13 2.25E-13 4.64E-15 G.OOE-13 l.SOE-13
J.z-!28/Jm 8.08E-16 9.00E-14 2.25E-14 4.93E-16 l.OOE-14 5.00E-15 5.01E-16 9.00E-13 2.25E-13 1.06E-14 6.00E-13 1.50&13
3/29}1999 2.0i>hl6 9.00E-14 2,25E-14 2.06E-16 l.OOE-14 5.00E-15 1.42E-16 9.00E-13 2.25E-13 6.69E-15 G.OOE-13 1.50E-13
7/3/1999 S31E-16 9.00E-14 2.25E-14 2.47E-16 2.00E-14 5.00E-15 2.23E-16 9.00E-13 l.25E-13 6.44E-15 6.00E-13 l.SOE-13
9/21/1$9 8.!18&-16 9.00E-14 2.25E-14 3.90E-16 2.00E-14 S.OOE-15 2.96E-16 9.00E·13 2.25E-13 7.29E-15 6.00E-13 1.50E-13
11./28/1999 L48E-1S 9.00E-14 2.25E-14 6.00E-16 2.00E-14 S.OOE-15 5.57E-16 9.00E-13 2.25E-13 6.19E-15 6.00E-13 1.50E-13
~/21/2DOO 1.001'.·16 9.00E-14 2.25E-14 1.06E-16 2.00E·14 S.ODE-15 1.00E-16 9.00E-13 2.25E-13 6.23E-15 p.OOE-13 1.50E-13
6/26/2()00 3.47E-16 9.00E-14 2.25E-14 3.46E-16 2.00E-14 S.OOE-15 3.62E-16 9.00E-13 2.25E-13 4.50E-15 61!0W.3 1.50E-13
9/26/'1.000 2.51E-16 9.00E-14 2.25E-14 1.78E-16 2.00E-14 5.00E-15 3.25E-16 9.00E-13 2.25E·13 8.55E-15 fi.DOE-13 1.50E-13
0./~6/2000 1.00E-16 9.00E-14 2.25E-14 1.42E-16 2.00E-14 5.00E-15 1.31E-16 9.00E·13 2.25E-13 7.77E-15 6.00E-13 1.50E-13
~/26/.200~ 3.10E-16 9.00E-14 2.25E-14 l.OOE-15 2.00E-14 5.00E-15 l.OOE-15 9.00E-13 2.25E-13 7.19E-15 6.00E-13 1.50E-13
7{2.9/2001 1.52E-16 g,OOE-14 2.25E·14 1.44E-16 2.00E-14 5.00E-15 1.77E-16 9.00E-13 2,25E-13 7.21E-15 6.00E-13 1.50E-13
9/24/2001 1.03E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 .LOOE-16 9.00E-13 2.25E·13 8.09E-15 6.00E-13 1.50E-13
l2/:ll/20bl l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.39E-15 6.00E-13 1.50E-13
4/1/2002 2.05E-16 9.00E-14 2.25E-14 2.44E-16 2.00E-14 5.00E-15 2.29E-16 9.00E-13 2.25E-13 8.15E-15 6.00E-13 1.50E-13
?/1/2002 3.55.£·16 9.00E-14 2,25E-14 4.85E-16 2.00E-14 S.OOE-15 1.06E-16 9.00E-13 2.25E-13 7.65E-15 6.00E·l3 1,50E-13
9/30/200.2 Ll7E-16 9.00E-14 2.25E-14 1.61E-16 2.00E-14 S.OOE-15 1.00E-16 9.0DE-13 2.25E-13 3.68E-15 G.OOE-13 1.50E-13
12/30/2002 1.00E-16 9.00E-14 2.25E-14 1.03E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 9.46E-15 fi.OOE-13 1.50E-13
3/31/l003 1.20E-16 9.00E-14 2.25E-14 1.12E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 4.68E-15 6.00E·B 150R·.l3
6130/2003 2.18E-16 9,00E-14 2.25E-14 3.40E-16 l.OOE-14 5,00E-15 1.67E-16 9.00E-13 2.25E-13 5.96E-15 6.00E-13 l.50E-13
9/2~/2003 1.00E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.28E-15 6.00E-13 1.50E-13
1:1./29/2003 1.00E-16 9.00E-14 2.25E-14 2.54E-16 2.00E-14 5.00E-15 3.35E-16 9,0DE-13 2.25E-13 6.25E-15 6.00E-13 1.506·13
3/29/2004 l .OOE-1.1> 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.54E-14 6.00E-13 l.SOl:-13
6121/W04 1.~·1.6 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 3.04E-15 6.00E-13 1.50E-13
9/27/2004 l..OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.05E-14 6.00E-13 1.50E-13
U/'1.7/2004 1.Q_OE·l6 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 l,OOE-16 9.00E-13 2.25E-13 1.59E-14 6.00E-13 1.50E-13
3/28/2005 1.00E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 7.42E-15 6.00E-13 1.50E-13
6/29/~005 1.00E-16 9,00E-14 2.25E-14 1.30E-16 2.00E-14 5.00E-15 1.20E-16 9.00f.13 2.25E-13 7.94E-15 G.OOE-13 1.50E-13
9/·26/2005 l.OOE-16 9.00E-14 2.25E-14 1.56E-16 2.00E-14 5.00E-15 2.42E-16 9.00E-13 2.25E-13 1.22E-14 li.OIJE-13 1.50[·13
1/3/2006 2.!3£-1.6 9.00E-14 2.25E-14 1.04E-16 2.00E-14 S,OOE-15 l.OOE-16 9.00E-13 2.25E-13 3.73E-14 6.00E-13 1.50E-13
_4/3/2006 1.62E-16 9.00E-14 ~.25E-14 1.86E-16 ~.OOE-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 8.36E-15 6.00E-13 1.50E-13
7}~/2.006 1.86E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9,00E-13 2.25E-13 9_77E-15 6.00E-13 1.50£--u
10/2/2005 1.00E-16 g.OOE-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.30E-14 6.00E-13 1.50E-13
l./J./2007 1.00E-16 9.00E-14 2,25E-14 1.47E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.17E-14 6.00E-13 1.50E-13
~1moo1 2.l3E-16 9,00E-14 2.25E-14 1.63E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.65E-14 6.00E-13 1.50E-13
7!2/2007 3.35&-16 9.00<·14 2.25E-14 1.34E-16 2.00E-14 S.OOE-15 1.36E-16 9.00E-13 2.25E-13 1.78E·14 6.00~-13 1.50E-13
'J/30/2001 1.15E-16 9.00E·14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 7,68E-15 6.00E•l3 1.50E-13
lZ/31/2007 l.OOE':l6 9.DDE-14 2.25E-14 1..93£-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.31E-14 fi.OOE-13 l.50E·U
.3/ll/2008 1.14E-16 9.00E-14 '2.25E-14 U 3E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.44E-15 6.00E·l3 1.50E-13
~2008_ 7.C!IE-l6 -!l.ClOt-14 .2.25E-14 3.83.£-1'6 --2.00E-14 S.OOE·lS 2.27E-16 -9.00E·13 2.25E-13 6.52E-15 6~0£.'13 1.50E-13
Date Effluent Concentration Limit= BE-14 uCi/ml BHV-1U Effl"ent Concentration Limit = 2E-l~ uCl/ml BHV-lT Effluent Concentration Limit= 9E-13 uCl/ml BHV-lR Effluent Concentration Limit= 6E-13 uCl/ml BHV-1PB
lil.ARAGoal = Z.25E-14 uCi/ml Al.AAA Goal = SE-13 uCITml AI.ARA Goal -2..25£-13 uCljml IAlARA Go..l = l.SE-13 uCflml
Pre 1994 MPC Limit= SE-12 uCi/ml ,Pre 1994 MPC Limit= BE-14 .uCI/ml Pre 1994 MPC Limit= ZE-12 uCi/ml I.Pre 1994 MPC Limit= 4E-12 uCi/ml
Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 A LARA GOAL= 1E-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
9/30/2008 7.69E-16 9.00E-14 2.25E-14 2.94E-16 2.00E-14 5.00E-15 1.90E-16 9.00E-13 2.25E-13 7.64E-15 6.00E-13 l.SOE-13
12/31/2008 1.21E-15 9.00E-14 2.25E-14 4.76E-16 2.00E-14 5.00E-15 3.34E-16 9.00E-13 2.25E-13 1..16E-14 6.00E-13 1.50E-13
3/15/2009 2.14E-15 9.00E-14 2.25E-14 1.02E-15 2.00E-14 S.OOE-15 l.OOE-15 9.00E-13 2.25E-13 4~4£-l.S 6.00E-13 1.50E-13
6/15/2009 5.97E-17 9.00E-14 2.25E-14 2.35E-16 2.00E-14 S.OOE-15 2.18E-16 9.00E-13 2.25E-13 5.13E-15 6.00E-13 1.50E-13
9/15/2009 9.SSE-1.6 9.0010-14 2.25E-14 1.71E-16 2.00E-14 5.00E-15 9.87E-17 9.00E-13 2.25E-13 9.47E-1S 6.00E-13 1.50E-13
12/15/2009 1.241:-.15 9.1lj)E-J4 2.25E-14 9.25E-17 l.OOE-t4 S.OOE-15 S.WE"-17 MOE.-13 2.2SE'-l.3 5.9SS.l5 li.OOE-B 1.50E-13
Sl~1/20l0 1.97E-15 9.00E-14 2.25E-14 2..15E-16 1.1JPE·14 SJ)OE-15 3...27£•16 !l.!JOE-13 2.25E-l3 1.00E-14 6.00E-13 :t.Sil~13
6/30/2010 1.58E-15 9.00E-14 2.25E-14 4.71E--16 2.00£-14 S.OOE-15 7,70E-16 9.00E-U 2.25E-13 4.07£'-15 6.00E-13 l.SOE,13
9/lO/WlO 8:42£-16 9.00E-1~ 2.25E-14 2.80E-16 2.00f'-14 5.00E-15 1.31E-16 9.00E-13 2.25E-13 6.80E-15 6.00E-13 1.50EcU
V.{n/201.0 1..27E·l.S 9.00E-14 2.25E-14 2..3l.E-16 Z.OOE-M 5.00'E·1S 2.30E-16 $1.00E·13 l.25E-13 1.27E-14 6.00E-13 l.50E·l3
4/4/20U 9.01E"l6· ~.OOE-14 2.2SE-14 L90E-l6 2.006-14 S,OOE·l5 3.64E-16 9.00&13 2..25£.-U 1.09E-14 6.00E-13 :LSOE_-U
7/4/'lOU 1.59E-15 !I'.OOE-14 2.25E-l4 5.31E-l6 Z.OOE·lll S.OOE-.15 4.99E-16 9..00E·13 2..25£'-.13 8.38E-15 6.00E-13 l.SOE.-U
l0/3/20U 2..92£-16 9.00E-l4 2.2.SE-l4 U7E·l6 2.00Eo-1.4 5.00E-15 6.76E-17 9.00E-13 2,25E-13 1.14E·lll 6.00E-13 l5Cil·.13
l/3/20lZ 6.73E-16 9.00E·14 I!_25E'-l-t 1.19Y6 7.00&14 s.oo~-15 8.58E-17 ~.OOE·l3 2.25£.13 l..73E-14 6.00E-13 l..SOE·13
4/3/2012. 7.87E-16 9.00£-14 2.2SE.·lA 2.6111:-16 2.00£-111 5.DOE·15 3.95E-16 9.00£-13 2.2.SE-U L25E.l4 6.00E-13 l.sl>E-13.
Tfi/2012 1.86E-15 9.00E·14 2.25E-14 8.33(-.16 l ,OOE'·N S.OOE·15 9.85E-16 9.00E·13 2 .. 256-U 9.55&15 6.00E-13 l .SOE'·13
10/1/2012 1.061'-lS 9.00E-14 2.25E-14 2.11E-16 2.00E-14 5.00E-15 2.34E-16 l!-00£-13 2.25E-13 l.HE•l4 6.00E-13 1.50£·13.
12/31/2012 6.86<:-!6 9.00E-14 2.25E-14 1.27E-16 2.00E-14 5.00E-15 1.38E-16 9.00E-13 2.25E-13 1.54E-14 6.00E-13 1,50E-13
3/25/2013 9.91~16. 9.00E-14 2.25E-14 1.86E-16 2.00E-14 5.00E-15 2.04E-16 9.00E-13 2.25E-13 1.82E-14 6.00E-13 1.50E-13
7/2/2013 1.46E-16 9.00E-14 2.25E-14 3.34E-16 2.00E-14 5.00E-15 3.91E-16 9.00E-13 2.25E-13 5.78E-15 6.00E-13 1.50E-13
9/30/2013 8.89E-~6 9.00E-14 2.25E-14 9.13E-17 2.00E·l~ 5.00E-15 1.05E-16 9.00E-13 2.25E-13 8.00E-15 6.00E-13 1.50E-13
12/30/20Q_ S.21E.-1£ 9.00H4 2.25E-14 4.34E.·l7 2.00E-14 S.OOE-15 l.70E-17 MOE--1.3 2.25E-13 ~E~1~ 6.00E-13 l.SOE-13 ----·-------
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~ I« ~
~~~ ~ r. ~ b.. -,
~
I• t:t -....
-~ .. F--~
""" ,....
I UJ 0 0
(are:::rs 6o1)
1.!) (.0 ,.... ,....
I I UJ UJ 0 0 0 ~ ,.... ,....
-
-
-
-
-
-
-
1'-,....
I UJ 0 ~
s~-das
z~-das
~ ~-das
o~-das
6o-das
so-das
Lo-das
go-das
go-d as
vo-das
so-das
zo-das
w-das
oo-das
66-das
95-das
L6-das
95-das
95-das
v6-das
86-das
Z6-das
~5-das
o6-das
6e-das
ee-das
La-das
ge-das
gs-das
vs-das
se-das
zs-das
~e-das
TAB2
BHV-2 AIR SAMPLING GRAPHS AND DATA TABLE
Date Effluent Concentration limit = 9E-14 uCI/ml BHV-2U Effluent Concentration limit-2E-14 uCi/ml BHV-2T Effluent Concentration limit= 9E-13 uCi/ml BHV-2R Effluent Concentration limit-6E-13 uCi/ml BHV-2PB
AlARAGoal-2.25E-14 uCi/ml ALARA Goal-SE-13 uCi/ml ALARA Goal-2.25E-13 uCi/ml AlARAGoal-1.5E-13 uCi/ml
Pre 1994 MPC limit= SE-12 uCi/mi Pre 1994 MPC limit= SE-14 uCi/mi Pre 1994 MPC limit -lE-12 uCi/ml Pre 1994 MPC limit= 4E-12 uCi/mi
1.25E-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml I Pre 1994 ALARA GOAL=
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
9/l'i!>/1981 1.39E-15 S.OOE-12 1.25E-12 .3,69E-16 B,OOE-14 2.00E-14 5.92E-16 2.00E-12 S.OOE-13 1.67E-14 4.00E-12 l.OOE-12
12/14/1981 4.62E-16 S.OOE-12 1.25E-12 8.03E-16 B.OOE-14 2.00E-14 3.62E-16 2 OOE-12 S.OOE-13 1.33E-14 4.00E-12 l.PQE-12
3/29/1982 7.07E-16 5,00E-12 1.25E-12 1.10E-15 B.OOE-14 2.00E-14 7.27E-16 2.00E-12 S.OOE-13 1.52E-14 4.00E-12 l.OOE-12
6{30/l9~2 8.84€-16 5.00E-12 1.25E-12 7.73E-16 S.OOE-14 2.00E-14 4.78E-16 2.00E-12 5.00E-13 1.98E-14 4.00E-12 l.OOE-12
-9/77/1982 ·l:::DE-15 ,5.001!-12 1.25E-12 3.60E-16 B.OOE-14 2.00E-14 8.73E-16 2.00E-12 S.OOE-13 2;351:-14 4.00E-12 l.OOE-12
1/3/1!183 2.64E-15 5.00E-12 1.25E-12 2.55E-16 8.00E-14 2.00E-14 1.98E-16 .Z.OOE-12 !>.OOE-13 2.85E-14 4.00E-12 1.00E-12
4/4/JS83 2,14E-16 S.OOE-12 1.25E-12 1.02E-16 8.00E-14 :Z.OOE-14 1.57E-16 :Z.OOE-12 S.OOE-13 2.48E-14 4.00E-12 1.00E-12
6/30/1983 2..85E·l6 S.OOE-12 1.25E-12 2.06E-16 8,00E-14 Z.OOE-14 2.24E-16 Z.OOE-12 S.OOE-13 1.79E-14 4.00E-12 l.OOE-12
10/'3/1983 2.7Qf·l6 S.OOE-12 1.25E-12 3.36E-16 8.00E-14 2.00E-14 4.37E-16 2.00E-12 S.OOE-13 1.78E-14 4.00E-12 l.OOE-12
l/3/1984 2.78E-15 S.OOE-12 1.25E-12 1.20E-16 8.00E-14 2.00E-14 6.64E-17 2.00E-12 S.OOE-13 9.14E-15 4.00E-12 l.OOE-12
4/Vl98A 4.28E-16 5.00E-12 1.25E-12 1.75E-16 8.00E·14 2.00E-14 4.57E-17 2.00E-12 S.OOE-13 3.55E-14 4.00E-12 1.00E-12
7/2/1984 2.78E-15 S.OOE-12 1.25E-12 8.12E-16 8.00E-14 2.00E-14 1.98E-16 2.00E-12 S.OOE-13 1.68E-14 4.00E-12 l.OOE-12
JtJ/I/J!JS4 2.69E-16 S.OOE-12 1.25E-12 2.66E-17 8.00E-14 2.00E-14 O,OOE+OO 2.00E-12 5.00E-13 1.77E-14 4.00E-12 l.OOE-12
1/2/1985 2.15E-16 s.OOE-12 1.25E-12 7.55E-16 · B.OOE-14 2.00E-14 2.87E-16 2.00E-12 S.OOE-13 3.19E-14 4.00E-12 l.OOE-12
4{l/l!38S 1.00E-16 S,OOE-12 1.25E-12 1.67E-16 8.00E-14 2.00E-14 6.75E-17 2.00E-12 S,OOE-13 7.56E-15 4.00E-12 l.OOE-12
7/1/1985 3.70E-17 S.OOE-12 1.25E-12 9.00E-16 8.00E-14 2.00E-14 4.90E-17 2.00E-12 5.00E-13 1.31E-14 4.00E-12 l.OOE-12
9/30/1985 8.32E-17 S.OOE-12 1.25E-12 2.18E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 5.00E-13 3.64E-15 4.00E-12 l.OOE-12
l/2/19ll~ l-(XlE-16 S.OOE-12 1.25E-12 2.16E-16 8.00E-14 2.00E-14 2.15E-17 l.OOE-12 S.OOE-13 3.04E-16 4.00E-12 1.00E-12
4/1/1986 1.31E-15 S.OOE-12 1.25E-12 1.50E-16 8.00E-14 .2.00E-14 3.71E-16 2.00E-12 S.OOE-13 2.90E-15 4.00E-12 1.00E-12
6/30/198li 2.23E-16 5.00E-12 1.25E-12 1.32E-16 8,00E-14 2.00E-14 7.09E-17 2.00E-12 5.00E-13 2.53E-14 4.00E-12 l.OOE-12
10/27 /l!386 6.41E-16 5.00E-12 1.25E-12 1.74E-16 8.00E-14 ;!.OOE-14 3.67E-16 2.00E-12 S.OOE-13 1.04E-14 4.00E-12 1.00E-12
W.lS/1986 3.56E-16 S.OOE-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 1.05E-16 2.00E-12 5.00E-13 7.81E-15 4.00E-12 1.00E-12
3/lf>/1987 5.31E-16 S.OOE-12 1.25E-12 1.30E-16 S.OOE-14 2.00E-14 7.74E-17 2.00E-12 S.OOE-13 3.80E-14 4.00E-12 l.OOE-12
5/11/1987 4.06E-16 S.OOE-12 USE-12 6.63E-17 B.OOE-14 2.00E-14 1.34E-16 2.00E-12 5.00E-13 1.10E-14 4.00E-12 l.OOE-12
9/9/1987 2.74E-16 5.00E-12 1.25E-12 ,2.38E-16 l!.OOE-14 2.00E-14 1.38E-16 2.00E-12 5.00E-13 1.04E-14 4.00E-12 l.OOE-12
U/2/19S1 3.73E-16 6.00E-12 L25E-12 3.11E-16 B.OOE-14 2,00E-14 1.83E-16 2.00E-12 S.OOE-13 1.17E-14 4.00E-12 l.OOE-12
2/16/.1988 2.78E-15 5.00E-12 1.25E-12 2.31E-17 B,OOE-14 2.00E-14 1.20E-16 2.00E-12 S.OOE-13 3.55E-14 4.00E-12 l.OOE-12
5/18/tsBS 4.63E-16 S.OOE-12 1.25E-12 1.49E-16 8.00E-14 2.00E-14 2.30E-16 2.00E-12 5.00E-13 1.18E-14 4.00E-12 l.OOE-12
8/15/1988 8.06E-16 5.00E-12 1.25E-12 8.69E-16 8.00E-14 2.00E-14 1.80E-16 2.00E-12 S.OOE-13 1.42E-14 4.00E-12 l.OOE-12
1'1/14/1988 4.34E-16 S.OOE-12 1.25E-12 6.76E-16 8.00E-14 2.00E-14 1,57E-16 2.00E-12 5.00E-13 2.25E-14 4.00E-12 l.OOE-12
2/13/1989 5.80E-16 S.OOE-12 1.25E-12 2.85E-16 8.00E-14 2.00E-14 1.55E-16 2.00E-12 S.OOE-13 2.80E-14 4.00E-12 1,00E-12
5/15/1989 5.06E-16 S.OOE-12 1.25E-12 2.28E-16 8.00E-14 2.00E-14 1.63E-16 2.00E-12 S.OOE-13 6.05E-15 4.00E-12 1.00E-12
8/14/1989 4.71E-16 S.OOE-12 1.25E-12 9.60E-16 8.00E-14 2.00E-14 1.26E-15 2.00E-12 S.OOE-13 6.65E-15 4.00E-12 1.00E-12
_11/13/1989 1.14E-15 S.OOE-12 1.25E-12 4.08E-16 8.00E-14 2.00E-14 4.18E-16 l.OOE-12 S.OOE-13 1.59E-14 4.00E-12 1,00E-12
2/U/1990 1.09E-15 S.OOE-12 1.25E-12 3.25E-16 8.00E-14 2.00E-14 3.74E-16 2.00E-12 S.OOE-13 1.98E-14 4.00E-12 1.00E-12
S/14/1990 9.32E-16 S.OOE-12 1.25E-12 5.27E-16 8.00E-14 2.00E-14 3.97E-16 2.00E-12 S.OOE-13 1.69E-14 4.00E-12 l.OOE-12
8/13/1990 1.66E-16 5.00E·12 '1.25E-12 5.49E-16 S.OOE-14 2.00E-14 4.75E-17 2.00E-12 S.OOE-13 1.27E-15 4.00E-12 l .OOE-12
11/12/1990 6.05E-16 S.OOE-12 1.25E-12 2.64E-16 S.OOE-14 2.00E-14 1.93E-16 2.00E-12 5.00E-13 2.25E-14 4,00E-12 l.OOE-12
~ll/1.991 8.72E-17 S.OOE-12 1.25E-12 7.00E-18 8.00E-14 2.00E-14 3.33E-17 2,00E-12 5.00E-13 3.49E-14 4.00E-12 l.OOE-12
~/13/1991 1.16E-16 S.OOE-12 1.25E-12 3.86E-16 B.OOE-14 2.00E-14 2,80E-16 2.00E-12 S,OOE-13 1.50E-14 4.00E-12 l.OOE-12
8/12/1991 9.02E-17 S.OOE-12 1.25E-12 8.82E-17 S.OOE-14 2.00E-14 7.65E-17 2.00E-12 S.OOE-13 1.58E-14 4.00E-12 l.OOE-12
11/11/1991 4.81E-17 S.OOE-12 1.25E-12 3.82E-17 S.OOE-14 2.00E-14 2.54E-17 2,00E-12 S.OOE-13 1.45E-14 4.00E-12 l.OOE-12
2/10/1992 1.54E-16 5.00E-12 1.25E-12 6.82E-17 S.OOE-14 2.00E-14 1.40E-17 2.00E-12 S.OOE-13 3.41E-14 4.00E-12 l.OOE-12
5/11/1992 .2.38E-16 5.00E-12 1.25E-12 7.63E-17 8.00E-14 2.00E-14 3.07E-17 2.00E-12 S.OOE-13 1.27E-14 4.00E-12 l.OOE-12
8/10/1992 1.01E-16 5.00E-12 1,25E-12 7.07E-17 B.OOE-14 2.00E-14 2.80E-17 2.00E-12 S.OOE-13 1.41E-14 4.00E-12 l.OOE-12
11/9/1992 S.20E-17 S.OOE-12 1.25E-12 3.65E-17 8.00E-14 2.00E-14 1.78E-17 2.00E-12 S.OOE-13 1.71E-14 4.00E-12 1.00E-12
2/9/).993 2.39E-16 5.00E-12 1.25E-12 2.97E-17 8.00E-14 2.00E-14 6.31E-17 2.00E-12 S.OOE-13 3.41E-14 4.00E-12 1.00E-12
5/l0/1993 l.OOE-16 S.OOE-12 1.25E-12 7.11E-17 8.00E-14 2.00E-14 3.19E-17 2.00E-12 S.OOE-13 1.34E-14 4.00E-12 1.00E-12
8/.10/1993 1.90E-16 S.OOE-12 1.25E-12 l.OOE-16 8.00E-14 l .OOE-14 l.OOE-16 2.00E-12 S.OOE-13 1.80E-14 4.00E-12 l.OOE-12
11/8/1993 l.OOE-16 5.00E-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 5.00E-13 1.49E-14 4.00E-12 l.OOE-12
2/'1/.1994 2.23E-16 5.00E-12 1.25E-12 1.00E-16 8,00E-14 2.00E-14 1.84E-16 2.00E-12 5.00E-13 2.19E-14 4.00E-12 l.OOE-12
5/9/1994 2.16E-16 S,OOE-12 1.25E-12 7.20E-17 B.OOE-14 2.00E-14 9.89E-17 2.00E-12 S.OOE-13 1.37E-14 4.00E-12 l.OOE-12
8/9/1994 9,29E-17 6.00E-12 1.25E-12 2.96E-16 8 OOE-14 2.00E-14 3.04E-16 2.00E-12 S.OOE-13 l.OOE-16 4.00E-12 l.OOE-12
11/7/1994 9.21E-17 5.00E-12 1.25E-12 2.35E-16 B.OOE-14 2.00E-14 l.OOE-16 2.00E-12 5,00E-13 1,00E-16 4.00E-12 l.OOE-12 --
03~ Efflu.~nt Concentration Limit= 9E-14 uCJ/ml BHV-2U !Effluent Concentration Limit= 2E·14 llCi/ml BHV-ZT Efflu.ent Concentration limit= BE-.13 UO/ml BHV-~R Efflul!nt Concentration Limit= 6E-"l.3·UCT/ml BHV-2PB
Al.AAAGoal = 2:25E-14 uCI/ml ·AlARA Goal = SE-ll uCI/ml ALAMGoal= 2..2SE·l31d!l/ml ALARAGoal = l,SE-13 uCi/ml
Pre 1994 MPC Limit= 5£-12 uCi/ml Pni' 1994 MPC Limit = SE-14 uCifml Pre 1994 MPC Limit= 2E-12 uCi/!111 Pre 1994 MPC Umlt c 4E·12 uCi/ml
Pre 1994 ALARA GOAL= L25E-12 uCI/m1 Pre 1994 A LARA GOAL= SE-13 uCi/ml Pre 1994 A LARA GOAL= 1E-12 uCI/ml
Cone EFC EFCA Cone EFC EFC A cone EJ:c EKA C.o~e EFC EFCA
2/7/1995 1.18E-16 9.00E-14 2.25E-14 9.70E-17 2.00E-14 S.OOE-"15 9.70E·l7 !l.OOE-13 2.25t"l3 7.42E·15 6.®<'·13 1.50E-13
5/9/1995 9.40E-~7 !I.OOE·lll 2.25E-14 l.20E-l6 l .OOE-14 S.OOE-15 3.50E-16 9.00E-.19 .2.25E·13 ll.90f:.J5 li.POt•l3 LSOE-13,
8/9/1995 8.90E-17 9.00E-l4 2.25£·14 9.67E-17 2.lioE·l4 5.00E-15 1,35E-16 9.00E-B 2.25E-13 2.38E-16 6.00£-1..3 LSOE·B
11/11/1995 2.83£·15 !U:lO&lA 2.25E·14 4.c9&16 2.00[·14 5.00E-15 5.23E·16 9.00E-13 2.25E-13 6.77E-15 6.00E-13 ~ .. SOE-13
1/5/.J.'JSfi· 1.7SE·l5 9,00E·l~ 2.25E-14 8,66E-16 2.00E-14 .s.DO'E-lS 4.8~-16 9.00&13 2.2SE·l3 3.!l(IE-l5 G.OOE-13 1.50E-13
5/6/1996 1.40E-16 9.00E-14 2.25£·14 1.15~·16 ~-OOE-14 S:OOE-15 l.OOE-16 9.00£-13 2,25£•13 6.8SE-l!> 6.nQE·13 1.50E-13
8/$/1996 1.43E-16 9.0QE·l4 2.ZSE-14 2,78E-16 :l.()QE.,J4 S.OOE·is 1.00E-16 9.UGE-13 2.25(-13 SJUE·lS 61lOB3 1.501:·13
·ll/6/1996 1.45E-16 9JOOE·1of ~.isE-14 1.57E-16 2..00£-14 5.00E-15 1.00E-16 9.00£·13 2.25E-13 1.19E-14 6JlOE-ll 1.50£·13
2/6{1997 1.00£-16 9.oon-.L4 2.251:-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00N3 2.25E-13 S.84E.-16 6.00E-13 1.50E-13
·s/S/1997 l.!!Ot·16 !I.OOE-14 2.25E-14 1.00E-16 2.00E-14 5.001:·15 l .QOE-16 9.00E.-l3 2.25£·13 l.89E-15 6.00E-13 1.50E-13
Wll/19!17 1.00E·16 9.00E-14 1.25£,14 1.09E·l6 2.00~14 SJ)0£.15 l.OOE-16 9.00£-13 Z:2SE-13 5.69E·15 6.00&13 l.SOE-13
1/S/1998 2.55E-16 9.00<.-14 2.2SE-14 ~07E·l6 2.00E-14 5.00£-15 5.00E-17 9.00E·13 2.25E-13 5.l1E·l5 &,OOE.-13 1..50£·13
4/28/1998 UOE-16 9.ooE·14 2.25£·14 1.71E-16 UlOE-14 S.OOE-15 l.28E-16 9.00E-13 2.25E-13 6.40E-15 6.00E·13 1.SDE·l3
7/31/1998 1.47E-l6 9.00C~14 2.25E-14 4.24.E·l6 2.00E-14 S.OOE·lS 3,3SE-16 9:00E·l'3 2.25!:·1'3: 4.805-15 6.00E-13 1.50E·13
9/28ilS98 l .OOE-16 [9.00£·14 2.25E-14 l.QOE-16 2.00E-14 s.oo£-rs l .oot-16 9.QOE·13 2.25hl3 4.26E·l..S Ei:OOE-13 1.50E-13
l2/28jl99S 2.54E-16 9.00E--l4 2.2.SE·14 D5E-16 2.0QE·14 s:ooHs l.3BE·16 9.00E·l3 2.'25&13 6.88E-15 6.00E·l3 1.50£·13
3/29/.1999 1.07E-16 9.00E·14 2.'2.SE·l4 l .Oj)E-16 2.00E·1.~ 5.00E-15 1.00E·16 9.00Hl 2..25E-13 7.61E-15 6.00E"·l3 1.501:·13'
7/3/1999 2.46E·16 9.«!£:14 .USE-.14 l.OOE-16 2.ooe-.1A 5.00E-15 J.QO.E,.16 9.00E-13 2.25E-13 6.95E-15 6..00E·la l.SOF-13
9/27/l999 ?-.SlE-.16 9.00E'-l4 2.25E-14 1.41E-16 2.00E-14 S:00£·15 l.OOE-16 9.90£·'13 2.25E:H 7.35E-15 6.00E-13 1.50E-13
ll/28/1999 5'.20E·l6 9.00E-14 2.25£-14 2.60E-16 2.00E-14 S.OOE-15 2..01£-16 9.00EC13 2.25£-13 7.00E-15 6.00E'·l3 1.50E-13
3/27/2000 1.00E-16 9.1.l0E·l4 ·USE-14 l.OoE•16 2.001:"·14 S.OOE'-1!> l.OOE-16 9.00£-B 2.25E"·I3 7.12E-15 6.ooa-a l.SOE.,13
6/26/2000 1.10E-16 9.00M.~ 2.:l5£-14 l.OOF16 ~.OOE-14 5.00E-15 1.16E-16 9.00£;.13 USE-13 5,01E·l$ 6.00£·13 l.SOE-13
9/26/'1.000 UKlE.-16 ?.OOE-14 2.25E-14 1.00E-16 2.00£-111 5.00E-15 l.QQE-16 9.00E-13 2.25E-13 5.31E-15 &.OOE-13 l.SOE·B
12{26/2/XXJ 1.'261';-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE·15 LOOE-15 9,00£-13 2.2.SE·ll. 9.4SE,l5 6.00E-13 1.50E-13
?./26/2001' l.OO.E-~6 9;Q0E·l4 2.25E-14 1.00E-16 2.00E-14 S.O()E·IS 1.006·16 9.001?·13 2.2SE•lc3 6.9SE-15 6J)OE-t3 1.50E-13
7/2}2001 1.00E-16 9.00E.-l4 2.;15£-14 l.OOE-16 2.0(}f,-14 S.OilE•lS l.OOE-16 9.QOE-13 2.25E·U 6.56£•15 ~.OOl·U 1.50E-13
9/2.4/2001 1.00E-16 9.DOE:-14 2.25E-14 LOOE-16 z.OOE--14 5.00E-15 1.00E-16 9.00E·l3 2.25E-13 6.16E=IS 6.00E·13 l .SOE"-13
12/Sl/2001, l.OOE·iS 9.00E'·14 2.~E'-l4 1.00E-16 2.00E:·1.4 5.00E-15 l ,QOE.16 9.00£-13 2.25E-13 2.20E-15 6.00E·l3 l.SOE·13
4/1/2.002 l.lXlE-16 9.001!-14 2.25E-14 l.OOE-16 2.00E·14 5.00£-15 1.00£.1:6 9:001;-1'3 2.25(·13 9.9SE-1S 6.00E-13 1.50E-13
7/U~OOl 1.25E-16 9.00E-14 2.25E-14 1.43E-16 2.00E-14 S.OOE·~ l.OOH6 9.QOE·l3 2.25E·l3 s.25e~ts 6.00E-l3 1.50E-13
9130/2002 1.00E-16 9.00E-U 2.251'.·10 1.0010·16 l .OiiE-14 s.ool:-15 l.OOE-16 9.0Q::13 :t2~E-H H9E-15 6.00E-13 l.S0!:.-13
12/30/2.002 l.OOE-16 9.00f-14 2.2SE-14 l .OOE-16 2.0010-14 S.OOE-15 1,00E-16 s.ooe,n 2.25E-13 6;9lE·15 &.OOE-13 1.50!'-U
3/3l/200l l.OOE-1 6 9.00£·1~ 2.2SE.t4 1.00E-16 2.00E·l4 5.00E-15 l.OOE·16 9.00E-13 2.25E-13 6.16E-15 6.00E-13 l.S0£·13
&/30/2003 l.OOE.-16 9.QOE-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9,00!;-13 2:25£·13 5."270-lS 6.00£-13 l.SOE-13
9/29/2003 l.OOE-16 9.00E.·l4 2.25E-14 l.QOE-16 2.00E-14 5,00E-15 l .OOE-16 9.00E-13 2,25'£·13 7.23E-15 6.00i:-13 1.50£-13
12/29/2003 1.00E-16 9.00E-l4 US£-14 1.00E·16 2.00E·14 5.00E-15 l.OOE-16 9.0011·13 1.25E-13 7.80E-15 &.OOE-13 •1.50£·13
3/29/2904 1.00E-16 9.00E-l4 2:.25~·14 l .OOE-16 2 .. 00E·l4 5.00E-15 1.00£-16 !i.OOE-.13 2.25E-13 2.04E-14 6.00E·13 1.50£·13
'6/21/200A 1.00(·16 9JDOE·14 2,2SE-14 l.OOE-16 2.00E·l4 5.00E-15 l.OOhl& 9.00E-13 2,25E-13 3.09E-15 6.00E-13 1.50E-13
9{27/2004 l.OOE-lji 9.00E'14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.QOE-16 9.00E-U 2.25E.-13 1.73E-14 6.00E-13 1.50E-13
U/7:1/2004 l.OOE-16 9.00E-J4 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l .. DOE·l6 9.QOE-13 2.25£-13 130£·14 6.00E·l3 l.50E-13
3/28/2JJ(.)S 1.00E-16 9.001:'-14 '2.2-SE--14 L OOE-16 2.00E·l4 S.OOE-15 1,00£-16 9.001:.-'1.3 2.25E·I3 8.88E-l5 6,00E·l3 LSQE.·13
6(29/ZIJOS 1.00E-16 ~OOE-14 2.25E·l'l l.OOE•16 2._DOE·14 5.00E-15 l.OOE-16 9.DOE"·13 2.25E-13 s .. asf-15 6.00E·l3 LSOE'·H
9/26/200.~ 1.00E·l.6. 9.00E•l4 2.ZSE.-14 l.99E-16 2.00t•lit 5.00E-15 1.44(;-16 9.00E-13 2.25E-13 3.81E-14 6.00E-13 l.SOE·l3
lh/1006. l.291i-l6 9.00E.·14 2.25E-14 l.OOE-16 2.00E-14 5.00£·15 4.08E.ol6 9.0QE-13 2.2Sf·H 6..58£·1<1 6.00E-13 1.50E-13
4/3/2006 1.02E-16 9.001:-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 l ,OOE-16 fi.OOf-13 2.25"£-13 .1.08E·I4 6.00E-,13 1.50E-13
7/3/2006 1.00E-16 9.00E-14 2-lSE-14 LOOE·16 2.00E·14 S.OOE·15 1.00E-16 9.00E-J3 2.2SE-13 UOE-1<1 &.OO_E-13 l.SOE-13
10/Zilo~6 1.30E-16 9.00E-14 2-ZSE-14 l.OOE·16 2.QOE-14 S.OOE-15 1.00E-16 9.0Ce·13 2.25£-:13 1.68E-14 6.00&-13 l.SOE·l3
1/-V?.fxl7 l .2.4E-16. 9.00E·l4 u .sr-1.; 1,00E-16 2.00E-:14 5.00E-15 l:QOE.-16 9.00E-13 2.25E-13 l.38E-14 6.00E-13 l.50E-13
11/2{2007 lAOE-16 9.00£-.N 2.25E-14 1.00E-16 2.00E·14 S.OOE~ l.OOE-1:6 9.00E·l3 :USE-13 L63E.·l4 6.00E-13 1.50E-13
7/2/2007 1.04E-16 9,00E-14 2.25E-14 l.OOE·lfi 2.00E-14 5.00~-15 l._ooE-16 9JlOE·l3 2.2St-19 U6E-14 S,OOE-1.3 l.50E-13
9/30/2007 l.OOE-16 9.00E·l4 7.:1Sf'·l4 1.00E-16 2.001!44 S.OOE:l.S l.OOE-16 9.00£-13 2.25E-13 324E-15 6.00E-13 1.50E-13
12/31/2007 1.91E-16 9.00E·14 2.2.SE.l4 1.00E·16 2.00E-14 5.00E-15 1,00E-16 9.00E·13 2.25E-13 1.18E-14 6.00£·13 l.SOE-13
3/YJtwoa l.OOE-16 9.00(·14 2.25E·l4 1.00E-16 2.00E·l4 5.00E-15 l.OPN6 9.00E-13 2.25E-13 6.49E-15 6.00E-13 1.50E-13
~0/2008 . -,g~.-16 . 9.00£-14 2.25E-14 1.00E-16 -2.00E-14 2-~-lS LOOE-16 9.00<·13 2.25E-B 4.82E-l.S 6.00E-13 1.50E-13 ----------
Date Effluent Concentration limit= 9E-14 uCi/ml BHV-2U Effluent Concentration Limit= 2E-14 uCI/ml BHV·2T Effluent Concentration limit= 9E·l3 ud/ml BHV-lll Effluent Concentration limit= 6E-13 uCi/ml BHV-2PB
AlARAGoal = 2.25E·14 uCi/ml ALARAGoal = SE-13 uCi/ml Al.ARAGoal = 2.25E-l3 uCifml AtARAGoal = 1.5E-13 uCi/ml
Pre 1994 MPC limit= SE-12 uCi/ml Pre 1994 MPC limit= SE-14 uCi/ml Pre 1994 MPC limit= 2E·U ud/ml Pre 1994 MPC limit= 4E-12 uCi/ml
Pre 1994 A LARA GOAL= 1.25E'12qCi/inl Pre 1994 A LARA GOAL= SE-13 uCi/ml Pre 1994 A LARA GOAL= lE-12 uCi/ml
Cone EFC EFCA Con' EfC EFCA Cone EFC EF.C"A Cone EFC EftA
9/30/2008 2.73E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OQ~·l5 I.OOE-16 9.00t•U 1.2liE-B s.aot-15 6.00E-13 1.50E-13
12/31/2008 5.71E-16 9.00E-14 2.25E-14 1.61E-16 l.OOE-14 S:OOE·l5 1..25E·16 9.00E-13 2.25€-13' 2.04E·111 6.00E-13 1.SOE-13
3/15/2009 3.96E-16 9.00E-14 2.25E-14 1.38E-16 2.00E-l 4 S.OOE-15 1.07E-16 9.00E-H 2.25H 3 4,8.1£-15 6.00E-13 1.50E-13
6/15/2009 1.24E-17 9.00E-14 2.25E-14 4.64E-17 2j){)f-1~ S,OOE-15 5.11E-17 9.j)OE-13 US£-13 458£·15 6.00E-13 1.SOE-13
9/15/2009 2.43.£·16 9.00E-14 2.25E-14 5.28E-17 2.00E-14 5.00E-15 4.84E-17 9.00E-13 2.2.5E-l3 1.19E-14 6.00E-13 1.50E-13
12/15/2009 5.72£-.16 9.00E-14 2.25E-14 2.94E-17 2..00E-lA SDOE-l.S 2.5n·17 9.QOE·l3 '2.25E·l3 6.70E·15 6.00E-13 1.SOE-13
3/31/2010 5.47£"16 9.00E-14 2.25E-14 1.42E-17 i.OQE-14 5.00E·15 11-.66£-17 9.00E-13 2.2~E·l3 8.24E·15 6.00E-13 1.50E-13
6/30/2010 3.SSJ>-.16 9.00E-14 2.25E-14 6.64E·l 7 2.00f·14 S.OQE-15 9.90£-11 9.00.E.·l3 2.25E-B 2.01E·lS 6.00E-13 1.50E-13
9/30/2010 2..!UE-16 9.00E-14 2.25E-14 4.48E'·l7 .2'.00E-14 S.Oil.E·lS 5.12E-l7 9.00E·l3 2.25&B Ul8E·l5 6.00E-13 1.SOE-13
12/31/2010 S.73E•l 6 9.00E-14 2.25E-14 '7.24E-17 2.00E'l4 5.00E-15 6.76E-17 9.00E-U 2.25E-.t3 1.35£-14 6.00E-13 1.SOE-13
4/4/2011 S.79E-16 9.00E-14 2.25E-14 4.01E-l7 2-QOE-'t~ 5.00E·15 9.llE-17> .9.ociE·13 2..2.5E-13 1 .. 06E-\4 6.00E-13 1.50E-13
7/4/2011 3.07E-16 9.00E-14 2.25E-14 8.54E-17 2.00E·l4 5.00E-15 !HlE-17 9.00E-13 2.25E-13 !7.21E-15 6,00£·13 1.50E-13
10/3/2011 l.llE-16 9.00E-14 2.25E-14 3.04E-17 2.00E·14 5.00E-15 2.81E·l7 9.00E-13 2.25E-13 1.03E-14 6.00E-13 1.50E-13
1/3/2012 3.65E-16 9.00E-14 2.25E-14 2.72E-17 2.00E-14 5.00E-15 4.S4E-.l.7 9.00E-13 2.25E-13 1.58E-14 6.00E-13 1.50E-13
4/3/2012 4.22E-16 9.00E-14 2.25E-14 1.15E-16 2.00E·.t<~ 5.00E-l5 2.77E-16 9.00E-13 2.25E-13 1..58E-14 6.00E-13 1.50E-13
7/2/2012 3.39E-16 9.00E-14 2.25E-14 1.56E-16 2.00E-14 5.00E-15 1.74E-16 9.00E-13 2.25E-13 8.60E-15 6.00E-13 1.50E-13
10/112012 3.13E-16 9.00E-14 2.25E-14 4 13E:,17 l .OOE-14 5.00E-15 3.04E-17 9.00E-13 2.25E·13 1.03E-14 6.00E-13 l,50E-13
12:fol/201Z 2.76E-16 9.00E-14 2.25E-14 5.41E'-l.7 2.00.~14 5.00E-15 7.05E-17 9.00E-13 2.25E-13 1.48E-14 6.00E-13 1.50E-13
3/25~2D13 3.38E-16 9.00E-14 2.25E-14 3.94E-l.7 LOOE-14 5.00E-15 8.32E-17 9.00E-13 2.25E-13 1.42E-14 6.00E-13 l.SOE-13
7f2/Wl3 4.06E-16 9.00E-14 2.25E-14 4,8Slf.17 2.pot-14 5.00E-15 8.06E-17 9,00E-13 2.25E-13 4.93E-15 G.OOE-13 1.50E-13
9/30/2013 1.76E-16 9.00E-14 2.25E-14 2.52D7 2.00E-14 5.00E-15 6.13E-17 9.00E-13 2.25E-13 4.90E-15 6.00E-13 1.50E-13
ll/30/2013 6.20E-16 ---·-~E-14 ___ 2.25E-14 ~.19E'-17 d-LXJE-!:4_ 5.00E-15 3.72E-17 9.00E-13 2.25E-13 2.50.E:=l4 6.00E-13 1.50E-13 ----------
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Effluent Concentration Limit= 9E-13 uCi/ml
ALARA Goal= 2.25E-13 uCi/ml BHV-2 Radium-226 Concentrations (uCi/ml)
Pre 1994 MPC Limit= 2E-12uCi/ml
Pre 1994 ALARA Goal -= SE-13 uCi/ml
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TAB3
BHV-3 AIR SAMPLING GRAPHS AND DATA TABLE
Da.te Effluent Concentration Limit =-9E-.14 uCi{ml BHV-3U EfflueJtt Concentration Limit= 2E-14 uCl/ml BHV·3T Etnuent Concentration Limit a 9E-13 uCl/ml 8HV-3R Efflut!lll Concentration Limit = 6E·13 ~Cl/ml BHV-3PB;
ALARA· Goal -2.2SE·1411C'"I/ml AU\RAGoal = S"E-13 uCI/ml AU\RAGoal= 2,25"E-13 uCI/ml ALARAGoal= l.SE-13 uCi/ml
Pre 1994 MPC Limit= Sf'=lZuCi/ml Pre 1994 MPC Limit= SE-14 uO/ml Pre 1994 MPC Limit= 2E·l2 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml
Pre.l994 ALARA GOAL: 1.25E-12 uCi/inl Pre 1994 ALARA GOAL = .SE-13 uCI/ml Pre 1994 ALARA GOAL = fl_E-tz.uO/ml
Cone f;J'C EFCA con" m: EFCA Cone EFC EFCA Co~t EfC EfCA
9/'JB/1981 1.74E-15 S.OOE·U 1.25E-12 9.02E-Ui e.ocr-14 2.00E-14 2.87E·l6 2.00E-12 S.OOE-13 1.54E-14 4.00~12 1.oOE-l2
12/Wl9S1 1.59E-15 S.OOE-12 1.25E-12 5.03E'-l6 8.00E-14 2JXIE·14 130E-16 2.00B2 S.OOE-13' 2.2!iE,l<l 4.00E-12 1.00E-12 ,
3/'l!J/1982 3.76E-16 5.00E·l!2 L2SE·l2 s.tsE-16 S.OOE-1~ 2,00H4 4.0SE>16 2.00£-ll S.OOE'-13 1.96E-14 II.OOE•lZ. l.(lllE·U
6/39/'198z 3.113£-16 S.OOE-12 1.25E-12 2.16E-16 B..OOE•14 l .OOE-14 .1.41E-l5 2.QOE·l2 S.OOE-13 2.40E-14 4.00U2 LOOE·U
9/27/1981 5".95H6 S.OOE-12 1.25E-12 L44E-l5 8.00E-14 2.001;-]4 5.36F-16 2..00£·12 S.OOE'-.13 1.43£-14 4.00E-12 1.00E-12
l/311983 2.05E-16 s.ooe-u 1.2SE-U 1.23lt-16 S.OOE-14 2.00£-14 l.lOE-16 2.00£-12 S.OOE-13 3.01E·14 4.00W2 •l.OOt-'12
4/4/,1933 LOOE-16 S.OOE'-~2 1.25E-12 6.94·E-l.7 8.00E·l4 2.00E-14 6.ll517 2.00E-12 S.OOE-13 1.39E-14 4.00E-12 1.00H2
6/30/1983 3.06E-16 S.OOE-12 1.25E-12 9.S9E-17 8.00E-14 :Z.OOE-14 2.08E·l 6 z.OOE-'12. S.DOE-l.S 1.70E-14 4.00E-12 1.00E-12
10~/1933 1.91E-16 S'.OOE-12 1.25£·12 3.05E·16 8.00E·l4 2.00£,14 2.79E-16 2.00t-U s.OOE-13 1.76E-14 4..llOH2 1.oow2
1/3{.19.$4 a.on:-16 S.OO.E-12 1.25E-12 ~.51£,17 8.001!'-14 Z.OOE-14 l.OOE-16 2.00£-12 S.OOE-13 9.17E-15 4.00E-l2 l.OOE-12
4};2/1984 8.22E-lli S.OOE-12 1.25E-12 7.52E-16 8.00£-14 2.00E·14 s.zoii-17 2.00E'·12. S.OOE-13 M7M4 4.00£-12 1.00E-12
7/-21.1984 5.29E-16 5.00~·12 L2SE-l2 G.18E-16 8,J)OE-l4 2.00E,14 1.40E-16 MOE•U S.OOE-tl 1.32E-14 •!.OOE•12 l.OQE-12.
l0/l/l984 1.74£-16 S.OOE·U 1.25E-12 7.10E-17 S.OOE-1.4 2.00E-14 l.OO.E-16 2.00E-12 S.OOE-13 1.08E-14 4.00E·U l.OOE-12
1/2/1985 1.00£-17 S.OOE-12 1.25E-12 7.10£·17 8.00£-14 2.00£-14 7.80E-17 2.()0£.-1.2. S.OOE-13 2.73£-14 4.00E-12 l.OOE-12
4/l/1985 1.00E-16 S.OOE-)2 L2SE-12 2.76E·16 B.OOE-14 2.POE-14 4.10E-17 2.001!-12 S.'OOE·U 1.12E-14 4.00E·l2 1.00£-12
7/1/1985 ~.04[,16 S.OOM2 1,25E-12 1.00E-16 ~E-.14 2.00E-14 ·l.OOE-16 2.00E-12 S.OOE-13 1.64E-14 <I.OOE'-12. l.OOE-q
9/30/1985 l.OOE-16 S.OOE-12 1.2SE-12 t.QOE-15 8.00E-14 2.00E-14 lJ)OE.-1.6 l.OOE-12 S.OOE.-13 1.73E-14 4.00Sl2 l.OOE-12
ll2i!SZ6 1.03E·15 S.OOE-U 1.2SE·l2 3.17E-16 8Jl(lf-f4 2.00&14 1.25E-16 2.00&12 S.OOE-13 1.21E-17 4-tlOE-12 1.00E-12
4/1/lS86 &04fi-15 S.OOE-12 1.25E-12 1.93E-17 S.OOE-14 2.00E-14 1.54E.-.16 2.00E·12 S.OOE-13 1.69E-14 4.00E-12 l.OOE-12
G{30/198ii 4.29£-!6 S,OOE-12 1.25E·12 1.77E-16 8.00E-14 2.00E·14 z.sae-16 :tOOE-12 S.OOE-13 1.97E·l4 4.ooe-u 1.00E·12
10/27/1986 6.45E-16 S.OOE-12 1.2SE·l2 9.8&1£-"11· S.OOE-14 Z.OOE-14 4.16E-15 Z.OOE-12 5.00£-13 t.64E·l4 II.OOE·ll l.OOE-12
lZ/15/11186 1:31£-16 S.OOE-11 1.25E·12 O.OOE-!-00 a.ooE-14 2.00£-14 4.16E-17 2.00E-12 S.OOE-13 .UOE-.15 <~.OOE-12 .l.OOE-12
3/1.6/1987 2.0.1E·1G S.OOE-12 1.2SE-12 1.20£-16 8.00E-14 2.00~14 5.73£-17 2.00E·12 S.OOE-13 l.GOH~ 4.00"E-12 1.00E·12
5/ll/19,87 2.16E·16 s.ooe-u 1.2SE-12 L96E·l6 8.00&14 2.00E·l4 7.38E-17 2.00E-12 S.OOE-13 1.59E,1~ 4.00.E-12 l.OOE-12
9/9/1987 2.1lE-16 5.00£-.12 1.25E-12 U 8E-16 B.odE-14 2.00E-14 3.52E-17 2.00E-12 S.OOE-13 1.46E-14 4.00E:·U l.OOE-12
11/2/1987 2.,44E-Hi S.OOE-12 1.2SE-12 2.32E-16 B.OO"E-14 2.00E-14 2.37E-17 2.00E·.1"2 5,00&13 2..48E··1.4 4.00E·l2 l.OOE-12
2/16/1988 8.9BE-l.G ~.llPE.-12 1.25£-12 2.SSE·l6 8.00E•l4 2.00E-14 3.42fol6 2.00C'·12 S.OOE-13 5.61£-14 4.00E·l2 1,00E-12
S/18/.1983 l.14E-16 S.OOE-12 1.25E·12 4.14!:·1-7 S.OOE:-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 1.20E-14 ~.OOE·ll 1.00E-12
B/15i1988 2.08E-16 S.OOE-12 1.25E-12 3.06E-16 &00£·14 2.00E-14 3.6SE-17 2.00E-12 S.OOE-13 1.36E-14 4.005-U l.OOE-12
11/14/1988 4.21E-16 S.OOE-12 1.25E·l2 2.93£-16 8.00E·l4 2.00E-14 1.09E-16 2.00E-12 S.OOE.-13 2.48E·14 oi..OO.E.-12 l.OOE-12
2/13/1989 4.4Sa-.16 5.oOE'-l2 l.25E·U 4.78E-17 S.OOE-111 2.00E-14 2.47E-17 2.00E-12 S.OOE-l3 l34E·.14 4.00~1:! l.OOE-12
~/15/.1989 l.O~E'-16 S.OOE-12 1.25E-12 1.00E-16 8.00E-14 2.00E-14 V 15E·17 2.00E-12 S.OOE-13 6.56E-15 4.00£-12 l.OOE-12
8/Wl989 1.31E-16 S.OOE-12 1.25E-12 S'.SSE-17 .8.00E·l4 2.001:·14 3.97E-1·7 Z.OOE-12 S.OOE-13 6.75E-15 4.00E-12 1.00E-12
11/13/1989 t.67F·l6 S.OOE-12 l-_25£·12 3..S7E-1'7 S.OOE-14 2.00E-14 8.03E-17 2.00E-12 S.OOE-13 1.69E-14 4;00[·12 l ,OOE-12
2/ll/1990 4:43£C16 S.OOE-12 1.25E-12 1.00E-16 8.00E·14 2.ooE-14 3.SOE-17 2.00E-12 S.OOE-13 2.37E-14 4,00E·ll l.OOE-12
5/14/1990 3.84E-16 S.OOE-12 .USE-12 2.54&16 8.00£-14 2.00£·14 1.02E-l6 2.00E.'l2 5.001;-13 l.GSE-14 4.00E-12 1.00E·12
8/13/1990 7.27E-17 S.OOE.-12 1.2SE·12 M 7E-1G 8,()()£-14 2.00E-14 1.21E-17 z.ooe:-12 S.DOE-13 7.86E-15 4.00~-12 l.OOE·U
U/1·Z/1990 l.84E.·l6 5.00£-12 1.25E-12 1.34E-16 llOOE-14' 2.00E-14 8.53£-17 2.00E-12 S.OOE-13 2,01E-14 ~.OOE'·l2 l.OOE-12
2/11/1991 4.66E·17 S.OOE-12 t ,25E-12 8.4$E-lf> 8.00E-14 2.00E·l4 1.94£-17' 2.00£.,1.2 5.00£.·13 3.69<·14 4.00E-12 1.00E-12
5/13/1991 5.0~17 s.OO.E-12 1.2SE·l2 7.40E-17 lt00E'14 2.00E·l11 7.00£-18 2.00£'·12 5.00E·l~ l..~E.-1-1 11.ooe.,u 1.00E-12
8/'12/1991 7.14E-17 S.OOE-ll 1.25E-12 '6.2.2E·l7 8.00f·l.4 2.00E·14 7.9SE-17 2.00E-12 S.OOE-13 1.77E-14 4.00E.·U l.OOE-12
ll/11/1991 1.41E-17 S.OOE-12 1.25E-12 2..JSE-18 8.00£-14 2.00E-l4 2.75E-17 !l.OOE·1l S.OOE-13 1.18£-14 4.00E·12 1.00E-12
i/W/199'1. 8.12E·17 S:OOE·12 1.25E-12 23S:E·17 8.00(·14 2.00£·14 2.76E-18 Z.OOE-.12 5.00E·l.3 3.57E·l4 4.00£-12 l.OOE-12
S/J.l/1992 9.18E-17 S.1)0E-12. 1.25E·12 S..8CE·l7 S.OOE·lA 2.00E-14 J.ase.-u 2,00E·l2 S.OOE-13 1.28£-14 ~.OOE-12 l.OOE-12
8/10/1992 2.001:-18 S.OOE-12 1.25E-12 4.19£-17 8.00E·14 2.00E·.l4 2.00E-18 2..00£·12 S.OOE·13 1.59£-14 4.00£-12 l.OOE-12
U/\ll1992 4.00E·l 7 S.OOE-12 l.2SE·12 2.68£-17 a:OOE-14 2.GPE-14 1.07E·l7 Z.OOE-12 5.00£-13 l:SlE·14 4.00£-U l·:OOE·l2
mlm3 7.94E-17 S:OOE-12 1,25E-12 l.OOE-16 S.()OE..14 2.00E-14 1.09£·16 2.00E-12 S.OOE-13 2.69E-14 •1.00!!-lL LOOE-ll
5/10/1993 1.60E-17 S.OOE-12 1.2SE-12 5.07E-17 8.00E-14 2.0()E-'14 7.64E-17 2.001:-'12 s:ooe-n •1.26E·l4 II.OOE·U 1.00E-12
8/10/1993 6.00E-17 S.O~E-12 l.2SE-l 2 o.OOE-l8 8.00£·14 2.0()E'-14 l.OOE-16 2.00£-12 s.OOE-13 ~14 4.C:Ofi-ll l.OOE-12
ll/8/1993 l,OOE-16 S.OOE·l2 1.25£-12 1.00E-16 8.00£-14 2.00E-14 1.00E·1,6 2.00E-12 S.OOE-13 2.10E-14 4.00f'·U l.OOE-12
2/7/1994 1.61E-16 S.OOE-12 1.2SE-12 1.00E-16 8.00E-14 l.OOE-14 2.22£•16' 2.00E-l2 S.OOE-13 2.23E-14 4.00E·12 l.OOE-12
5/!>/1994 2.77£-16 S,OOE·IZ usa-u 2.8QE-17 8.0()£-14 2.00E•lA 8.37E-18 2.00E-12 S.OOE-U 1.'lOE·l4 4.00E·12 l.OOE-12
8/9/199/l 7.39E-17 S.OOE·ll 1.2510-12 l.OOE-16 8.00E-'14 2.00E-14 1.14£·16 2.00E·12 S.OOE-13 l.OOE-16 4.00E-12 1.00£·12
Uf1/i!J94 !I.OSE-17 S.OOE-12 1.25E-12 1.00E-16 8.00E-14 2.00£·14 1,,00~·16 2.00£·12 s.ooE-13 l.OOE·l6 4.0QE·l2 1.00E-12
Date Effluent Concentration limit= 9E-14 UO/t;nl BHV-3U Effluent Concentration limit= 2E-14 uCi/ml BHV-31' Efthsent Concentration Limit= 9E-13 uCI/ml BtlV•3ft Effluent Concentration limit= 6E-13 uCi{ml BHV·3PB,
AI..AAAGoal = 2.25E-14 uCJ/ml AW,AGoal-SE·l3. LiC"I/ml ;cuARAGoal-USE-UuO/ml ALARAGoal = l.SE·UuCI/ml
Pre 1994 MPC limit= SE-Uudjml ·Pre.l994 MPC limit-se:JA uO/ml Pre 1994 MPC limit= 2.E·llu0/ml Pre 1994 MPC limit= 4E-U u<:r/m1
Pre 1994 ALARA GOAL= 1.25E-U uCi/<nl Pre 1994 ALARA GOAL= SE·13tlc:l/ml Pre 1994 ALARA GOAL= lE-12 uCi/ml
Co.hc tic EFCA Cone EFC £FCA cone EFC EI'C.A Cal)(; EFC £FC A
2nll'ffl'S 7.99E-17 9,00E'-l4 2.25E-14 9;60E-t7 2.00E-14 S.OOt-lS 9.60E-17 MOE-13 2.2SE·1J 9.05£·15 6.QOE-l3 1.50E-13
5/9/1995 9.40&-17 l!.00£·14 2.2SE-lA 9.90E-17 i.QqE-14 S.OOE-15. S.60E•17 9.00813 2.~~-.13 2.88£,-.15 6.00£-13 1.50~·13
8/9/1995 7.30E-17 9.oot:-t.: 2.isE·14 9.2ot-17 2.00E·14 5.00E-15 4-00E-17 9;00E-l3 2.25E-13 1.96E-15 ~.om:-13 I.S"Ot ·l3
U/11/1.995 3.16E-16 g·;OOE·lA 2..25E-14 l.31E-16 2.o<1E-14 5.00E-15 6.58E·17 9.00E-13 2.2.Sf-13 1..9ll·l4 6.00E-13 1.50E-13
2/5/1996 3.4lE·lfi 9.001:·14 2.25E-14 2.26E·16 2.00E-14 ~,OOE•lS 1.18£·16 9.00E·l3 2.2,SE•l3 2.69E-l4 6.00E.l3 1.50E-13
5/6/1996 1.31E-16 9.00E-14 2:ZSC-14 1.39E'·16 2.00E·U 5;00E•1S L82E-16 'lOOE~ll ~.25£·13 l.53E-14 6.00E·l3 1.50E-13
8/5/1996 3.00E-16 9.0j)E-14 2..2SE.-14 M'iE-16 MOE-14 5.00E-15 3.99E-16 9.00E·H 2.25E-13 1.31E-14 6.00E·13 1.50.E·13
11/6/1996 3.16£-16 9.00E·l<l 2.2%14 1.31E-16 2.00&14 5.00E-15 6.S8E-t7 9.00E-13 2.25E·13 1.91E-14 6.0010-13 1.50£.-13
2/6/1997 3.4U.l& 9.1)0£-14 2.2SE-14 2.26E-16 2.00E·14 S.OOE-.15 1.18E·16 9.QOE·l3 U5E-i3 2..69£-111 6.00E-13 1.50E-13
5/5/1997 1.31E-16 9.00E-14 2.25E-14 13'.lE·l6 2.00E-14 S.OOE-15 1.82E-16 9.00£.-13 2.25E-13 1:53E-14 S.OOE·U 1.50E-13
8/11/1997 3.00E-16 !llOO.J;.-14 2.25E-14 3.43E-16 2.0(1E·14 s.OOE-lS 3.99E·16 9;00£-13 2.2.SE-13 1.31E-14 6.00£-13 l.SOi:-13
1/S/l$$ 3.16E-16 9.00E'-1:4 2.25E-14 1.31E-16 2-00<·14 5.00E-15 6.58E-17 -!l.OOE·ll 2.25E-13 1.91E-14 6.00E-13 1.50E-13
4/28/1998 3.41E-16 9.00£-14 2.251:.-14 2.26E-16 2-00E-14 S,OOE-15 1.18E-16 9.00E·l3 2..2SE·l3 2.69E·lJI G.OOE-13 1.SOE-13
7/31/1998 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S.OO.E-15 l.~E-16 9.00E-13 2.25E·13 1.53E-14 G.OOE-13 1.50E-13
9/28/1998 3.00E-16 9.00E-14 z .. 25E·l~ 3.43£-16 2.0QE·l4 S.OOE-1.5 3.99£-16. 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13
12/.28/1998 3.16E-16 9.00E-14 2.2SE·l4 l~tt·~ 2.00E·l4 5.0oE-1S 6.58E·17 9.00E·13 2.25E-13 1.91E-14 6.00E-13 1.50E-13
~/29/-1999 MlE-16 9.00E-14 2.25E-14 2.26E-16 2.00E·14 5.00E-15 l.lBE-16 9.00E-13 2.25E-13 2.69E-14 G..ooe:u l.SOE-13
7/3~1999 UlE-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E·13 2.25E-13 1.53E-14 6,00E-13 1.50E-13
9/27/1999 ~.OOE·.16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E·13 2.25E-13 1.31E-14 G.OOE-13 1.50E-13
12/28/1999 3.16E-16 9.00E-14 2..25£·14 l.31E·16 2.00E-14 5.00E-15 &..SSE-17 9.00E·13 2.25E-13 1.91E-14 6.00E-13 1.50E-13
3/28/2000 3.41E-16 9.00E-14 2i2.5£·14 2.2fi£':16. 2.00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 G.OOE-13 1.50E-13
6}26/2000 1.31E-16 9.00E-14 2.&-~4 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13
9/26/2000 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.Oilf·lS 3.99e-ts 9.00E·13 2.25E-13 1.31E-14 6.00E-13 1.50E-13
12/26/2000 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 .9.00E-13 '2,25E-13 1.91E-14 6.00E-13 1.50E-13
3/26/2001 3.41E-16 9:001:-14 2..2.5E-14 2:26E·.16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2,25E-13 2.69E-14 6.00E-13 1.50E-13
7/2/2001 1.31E-16 iJ.OOE-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.QOE-13 1.506-13
9/24/2001 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S,OOE·lS 3 .. 99fo·l6 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13
12/31/2001 3.16E-16 9,00E-14 2.25E-14 1.31£·16 2.00£-14 5.00E·15 6.58£·17 9.00E-13 .2.2SE-13 1.91E-14 6.00E-13 1.50E-13
4/1/2002 3.41E-16 9.00E-14 2.25E-14 2.26E;16 2.00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E·14 &:OOE·H · 1.50E-13
7/1/2002 1.31E-16 9.00E-14 .2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-l3 2.2SE-13 1.53E·14 6.00E-13 1.50E-13
9/30/2002 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.2SE-13 1.31E·14 6.00E-13 1.SOE-13
12/30/2002 3.16E-16 9.00E-14 2.25E-14 1,31E-16 2.00E-14 S.OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E·14 6.00E-13 1.50E-13
3/31/2003 3.41E-16 9.00E-14 2.25E·14 2-26E·lf> 2.00E-14 5.00£·1S i.18E .. l6 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 1.50E-13
6/30/2003 1.31E·16 9.00E-14 2.25E-14 1.39E-16 l.OOE-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 1.53E·14 6,00E·B 'I.SOE·.l.J
9/29/2003 3.00E-16 9.00E-14 2.25E-14 3.43E-16 Z.OOE-14 5.00E·15 3.99E-16 9.00E-13 2.25E-13 1.31E·14 G.OOE-13 1.50E·13
12/29/2003 3.16E·16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E·15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 l.SOE-13
3/29/2004 M.lE-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 S.OOE-15 l.lSE-16 9.00E-13 2.2SE-13 2.69£-M 6.00E-13 1.SOE-13
6/27/2004 1.31E·16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 L.~E·l~ 6.00£-.13 1.50E·13
9/27/2004 3.00E·16 9.00E·l4 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.2SE-13 1.31E-14 6.006·13 1.50E·13
12/27/2004 i1.16E-16 9.00E-14 2.25E-14 1.31E-16 2.()(}f-14 5,00E-15 6.58E-17 9.00E-H 2.25E-13 1.91E-14 6.00E·13 1.50E·13
3/2a/ZQOS 3-41£-16 9.00E·14 2.25E-14 2.26E-16 2.00E-14 S.OOE-l5 1.18E-16 9.00£-.13 2.25E-13 2.69E·l4 6,00E-13 1.50E·13
W29/2Cos 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 s.OOE-15 1.82£·16 9.00E-l3 2.&-13 l.S3E·1.4 6.00£-13 1.50E·13
9/26/21XJS 3.00E-16 9.001:·1~ '2.2SE-l4' 3.43E-16 2.00£-14 S.OOE-1"5 3.99E·l6 .9 .. 00E-13 2.2St:·l3 l.31£-J.4 6.00£-13 1.SOE·13
1/3/2006 3.16E·1,G 9.00E.-l4. 2;2SE·l~ 1.31<·16 2.J)OE.lq 5.00E-15 6.58E-17 9,9oe:u 2..2.Sfol3 1.91E-14 6,00~-13 1.50E-13
4/3/l.Orl6 3..41E·l6 9.00E·14 2.2.5!'.·14 2.2fiE-l6 2.001:-1~ 5.00E-15 l.l8.E.·l6 9.00E-13 2,25E-13 2.69E-14 6.00E-13 1.50E-13
7}3/2006 l.31f-16 9.00£-14 2.25E-14 1.39E-16 2.00E-14 S.OOE-15 }:82£·16 9.00E-13 "Z.25E·l3 LS3E-14 6.00E·13 1.50E-13
lJJ/2/2006 3.00E-1S 9.00E-14 2.25E-14 3.43E·.16 2.00E-14 S,OOE-15 3.99E·16 9.00£-13 2.2.5E-13 l.llE-14 6.00E-13 1.50E-13
1/1/7.006 3.16E-16 9.00E·14 2.25E-l4 1.31E·16 2.00E·14 S.OOT:·JS 6.58E-17 9.00:·13 1.25E-Ia 1.91E-14 &.OOE-13 1.50E-13
4/2/2007 3A1E-16 9.00E-M 2.25E-14 2.26E·l6 2.00£,-14 S.OOE-15 1.18E-16 9.QOE-13 2.25E-13 2.69E-14 li.00£·13 l.SOE-13
7/2/.2.001 :UlE.-16 9.00£·1!1 2.25E-14 1.39E-16 2.00E-14 S.OOe-15 uu:-16 9.00£·13 2.25E-13 1.51~·14 6.00E-13 1.50E-13
9/30{2007 3.001::'16 .9.QOE·l4 2.25E-14 3.43E-16 2.00E-14 5.00£·15 3.99£-16 9.00E·l3 2.25£-13 l..llf-14 6.00E·l3 1.50E-13
U/ll/lf)/)7 3.16E-16 9.QOE-14 2.25E-14 ~lE-16 2.00£·1~ 5.00£·1.5 6.SB_E-17 9.00E·13 2.2SE-l3 1.9lE·l4 6.00E·13 1.50E-13
3/31}2008 3.41E-16 s.ooe-1.<~ 2.250:-14 2.26t-l6 2.00.£-14 5.00E-15 1.18E-16 9.00E·13 2.25E·l3 2.69E-14 6.00E·13 1.SOE-13
6/30/2008 l.31E·16 9.00£·14 2.25£-14 1.39E·16 2.00£-14 S.OOE-15 1.82£·16 9.00E·l3 2.25E·13 1.53E-14 6.00E-13 1.50E-13
Date Efflue11t Concentration Limit= 9E-14u0/ml BHii•3U Effluent Concentration Limit -2E·14 uCi/mJ BHV-3T Effluent Concentration Limit: 9E-13 uCl/mJ BHV-3R Effluent Concentration Limit:. 6E-Uu0/ml BHV-3PB
1\LARAGoal= 2.2:5£-14 uCI/ml IUARit Goal = SE-13 uCi{ml Ai.ARA Goal = i2.5E-l3 u.Cl/ml A.LARAGoal = 1.SE·l3 uCi/ml
Pre 1994 MPC Limit= SE-12 uCl/ml Pre 1994 MPC Limit= SE-14 uCl/ml Pre 1994 MPC Limit= 2E-12u0/ml Pre 1994 MPC Limit= 4£·12-uCI/ml
Pre 1994 ALARA GOAL = 1.25£-12 uCi/ml Pre 1994 ALARA GOAL = SE·UuCifml Pte 1994 ALARA GOAL = lE-12 uCi/ml
Cone EFC 'EFCA CD.ilc EFC EFCA Cone EFC EFCA Cone EFC EFCA
9/30/2008 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00£·15 3.99E-16 9.00E-13 2.25€-13 l.llE-H 6.00E-13 1.50E-13
12/31/2008 3.16E-16 9.00E-14 2.25E-14 Ui.E-l& 2.00E-14 S.OOE-15 6.58E-17 9,00E·l3 2.25E-13 1..91£.-.14 6.00E-13 1.50E·13
3/15/2009 ,3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.001:.-13 2.25E-13 .2.69E-l4 6.00£-13 1.50E-13
6/15/2009 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 U12E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13
9/15/2009 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E·13 ;2.25E-13 1.31£·1!1 6.00E-13 1.50E-13
12/15/2009 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9'001;-ll 2.25E-13 '1..91£-lA 6.00E-13 1.50E-13
,3/31/2010 3.41E-16 9.00E-14 2.25E-14 2.~_6Eo16 2.00E·14 5.001:'-!5 1.18E-16 9.00(·13' 2.25E-13 2.69E-14 6.00E-13 1.50E-13
6/30/2010 1.31£-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 l.82E-16 9.00£·13 2.25E-13 1.53E-14 6.00E-13 1.50E-13
9/30/2010 3.00E-16 9,00E-14 2.25E-14 3.43j;'-16 2.00E-14 S.OOE·lS 3.99E·l6 9.00E•!3 2:25£·13 1.31E-14 6.00E·13 1.50E-13
~2/31/2010 3.16E-16 9.00E·1<1 2..25E-14 1.31H'6 2.00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 G.OOE-13 1.50E-13
4/4/2011 3.41E-16 9,00E-14 2.25E-14 2.26E-16 2.00E.·1~ S.OOE·lS ·l.l8t·l6 9 .. 00E·13 2.25E-13 2.69E·.14 6.00E-13 1.50E-13
7/4/2011 1.31E-16 9.00E-14 2.25E-14 139f'-]); 2.00E-14 5.00E-15 1.82E·l6 9.00E-13 2.25E-13 1.53E-14 6.00E-13 l.SOE-13
10/~12011 3.00E-16 !UlOE-i4 2..256-14 3;4SE·l6 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.2SE-13 131E-14 6.00E-Il 1.50£.-13
1/3/2012 3.16E-16 9;00(·14 2.2SE·l 4 1.31E-16 2,00E-14 5.00E-15 5.58E·l7 9.00E-13 2.25E-13 1.91E-14 6.00&.13 1.50E·13
4/l/2()12 ~41£-lEi 9.lm-1A 2.25E-14 2.26E-16 2.00E-14 S.OOE·lS 1.18&16 9.00E-13 2.25E-13 .2.69E-14 I>.OOE-13 1.50E-13
7/2/'lat2 1.31E-16 9.00£-14 2.2.St·l4 L.39E·16 l.OQf;.-14 S.OOE-is 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00&13 l.SOE-13
10/1/2012 l.OOE-16 9:00E=l4 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3:99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E·13 l .SOE-ll
12/31/2012 3.l EiE·11i . 9.00E;14 2.25E-14 1.31E-16 2.00E-14 S.OOE-15 6.58£'·17 9.00Fl3 2.251:-13 l.9JE·lll 6.00E-13 1.50E-13
3{25/2013 3.41E-16 9.00E•l 4 USE·l4 2.26E-16 2.00E.~14 S.OOHS 1.18E-16 9:00E-13 2.25E-13 2.69£-14 6.00E·13 1.50E-13
7/2./2013 1.9lE·lG 9.00E·l4 2.25E-14 1.39E-16 2.00E-14 S.OOE-15 1.82E·l6 9.00E-13 2.25E-13 1.53E-14 6.00E-13 l.'SOE·l'l
9}30/201~ :t.OOt-16 9.00E·l.il 2.25E-14 3.43E-16 2.00E-14 S.OOE'·lS 3.99~-~6 9.00E·l 3 '2.:2SE-l 3 UtE·lt, 6.00E-13 1.50E-13
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TAB4
BHV-4 AIR SAMPLING GRAPHS AND DATA TABLE
Date Effluent Concentration limit= 9E-14 uCi}ml BHV-4U Effluent Concentration limit= 2E-14 uCi/ml BHV-4T Effluent Concentration limit = 9E-13 uCi/ml BHV-4R Effluent Concentration limit = 6E-13 uCi/ml ~HV-4PB
ALARA Goal= l.25E-14 uCi/ml ALARA Goal= SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml
Pri!1994MPCUmlt= SE-12 uCi/ml Pre 1994 MPC limit-BE-14 uCi/ml Pre 1994 MPC limit= 2E-12 uCi/ml Pre 1994 MPC limit= 4E-12 uCi/ml
Pre 1994 A LARA GOAL-1.25E-12 uCifml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 A LARA GOAL= 1E-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
9/28/1981 5.20E-15 S.OOE-12 1.25E-12 2.93E·15 8.00E-14 2.00E-14 2.74E-15 2.00E·12 5.00E-13 1.84E-14 4.00E-12 l.OOE-12
12/14/1981 4.53E-15 S.OOE-12 1.25E-12 1.78E-15 8.00E-14 2.00E-14 2.29E-15 2.00E-12 5.00E-13 2.54E-14 4.00E-12 1.00E-12
3/29/1982 1.06E-15 5.00E-12 1.25E-12 1.42E-14 8.00E-14 l.OOE-14 l.07E-15 :Z,OOE-12 S.OOE-13 2.31E-14 4.00E-12 1.00E-12
6/30/1982 6.03E-15 5.00E-12 1.25E-12 1.57E-14 8.00E-14 .2.00E-14 2.62E-15 ,2.00E-12 S.OOE-13 2.25E-14 4.00E-12 l.OOE-12
9/2.7/l!J~2 1.26E-14 5.00E-12 1.25E-12 7.58E-16 8.00E-14 '2.00E-14 5.35E-15 .2.00E-12 S.OOE-13 2.68E-14 4.00E-12 l.OOE-12
l/~!1.983 4.33E-15 5.00E-12 1.25E-12 6.52E-16 8.00E-14 2.00E-14 6.04E-16 2.00E-12 S.OOE-13 2.57E-14 4.00E-12 1.00E-12
4/4/lS$3 1.25E-15 5.00E-12 1.25E-12 7.17E-16 8.00E-14 2.00E-14 6.76E-16 2.00E-12 S.OOE-13 2.00E-14 4.00E-12 1.00E-12
6/30/1983 3.73E-16 5.00E-12 1.25E-12 9.43E-16 8.00E-14 2.00E-14 4.13E-16 2.00E-12 S.OOE-13 l.20E-14 4.00E-12 l.OOE-12
10/3/1383 2.54E-16 S.OOE-12 1.25E-12 1.51E-16 B.OOE-14 2.00E-14 2.65E-16 2.00E-12 5.00E-13 2.SOE-14 4.00E-12 l.OOE-12
1/3/1984 2.76E-15 5.00E-12 1.25E-12 1.60E-16 8.00E-14 2.00E-14 1.05E-16 2.00E-12 S.OOE-13 1.59E-16 4.00E-12 l.OOE-12
4/2/1984 4.27E-16 5.00E-12 1.25E-12 2.33E-16 !!.OOE-14 2,00E-14 6.28E-16 2.00E-12 S.OOE-13 3.67E-14 4.00E-12 l.OOE-12
7/2/1984 2.57E-15 S.OOE-12 1.25E-12 1.36E-16 B.OOE-14 2,00E-14 l.llE-16 2.00E-12 S.OOE-13 1.58E-14 4.00E-12 'l.OOE-12
10/1/1984 4.18E-16 S.OOE-12 1.25E-12 3.54E-16 B.OOE-14 2.00E-14 1,10E-17 2.00E-12 5.00E-13 9.83E-15 4.00E-12 l.OOE-12
1/2/1985 S.30E-17 5.00E-12 1.25E-12 3.55E-17 8,00E-14 2.00E-14 7.00E-18 2.00E-12 S.OOE-13 2.57E-14 4.00E-12 l.OOE-12
4/1/1985 l.OOE-16 S.OOE-12 1.25E-12 6.00E-16 8.00E-14 2.00E-14 4.35E-17 2.00E-12 5.00E-13 5.02E-15 4,00E-12 l.OOE-12
7/1/1985 9.36E-16 S.OOE-12 1.25E-12 2,33E-16 S.OOE-14 2.00E-14 i.36E-16 2.00E-12 5.00E-13 7.48E-15 4.00E-12 l.OOE-12
9/30/1985 1.46E-15 S.OOE-12 1.25E-12 7.69E-16 8.00E-14 2.00E-14 5,38E-16 2.00E-12 5.00E-13 7 .. 86E-15 4.00E-12 l.OOE-12
1/2/1986 8.40E-15 S.OOE-12 1.25E-12 7.60E-16 8.00E-14 2.00E-14 1.99E-16 2.00E-12 5.00E-13 2.12E-14 4.00E-12 l.OOE-12
4/1/1986 5.79E-15 5.00E-12 1.25E-12 5.80E-16 8.00E-14 2.00E-14 1.34E-15 2.00E·12 5.00E-13 1.33E-14 4.00E-12 l.OOE-12
6/30/l986 5.19E-15 5.00E-12 1.25E-12 7.83E-16 8.00E-14 2.00E-14 2.20E-15 2.00E·12 S.OOE-13 7.14E-16 4.00E-12 " 1.00E-12
10/27/1986 11.60E-15 5.00E-12 1.25E-12 4.67E-16 8.00E-14 2.00E-14 2.37E-15 2.00E-12 S.OOE-13 l .BE-14 4.00E-12 l.OOE-12
12/15/1986 2.75E-15 5.00E-12 1.25E-12 5.90E-16 8,00E-14 2.00E-14 9.39E-16 2.00E-12 S.OOE-13 1.20E-14 4.00E-12 l.OOE-12
3/16/1987 4.64E-15 5.00E-12 1.25E-12 1.18E-15 8.00E-14 2.00E-14 4.97E-16 2.00E-12 5.00E-13 5.89E-14 4.00E-12 l.OOE-12
5}11/1987 4.35E-15 5.00E-12 1.25E-12 1.23E-14 8.00E-14 2.00E-14 1.13E-15 2.00E-12 5.00E-13 2.21E-14 4,00E-12 1.00E-12
9/9/1987 6.39E-15 5.00E-12 1.25E-12 1.50E-14 8.00E-14 2.00E-14 2.26E-15 2.00E-12 S.OOE-13 1.57E-14 4.00E-12 1.00E-12
11/2/1987 6.72E-15 5.00E-12 1.25E-12 4.53E-16 8.00E-14 2.00E-14 2.20E-15 2.00E-12 .S.OOE-13 2.55E-14 4.00E-12 l.OOE-12
2/16/1988 1.91E-15 S.OOE-12 1.25E-12 1.35E-14 8.00E-14 2.00E-14 11.42E-16 2.00E-12 .S.OOE-13 4.44E-14 4.00E-12 1.00E-12
5/18/1988 1.78E-14 S.OOE-12 1.25E-12 4.39E-14 S.OOE-14 2.00E-14 4.92E-16 2.00E-12 5.00E-13 1.38E-14 4.00E-12 1.00E-12
8/15/1988 7.56E-15 5.00E-12 1.25E-12 3.31E-14 8.00E-14 2.00E-14 1.51E-15 2.00E-12 5.00E-13 1.97E-14 4.00E-12 l.OOE-12
11/14/1988 1.47E-14 S.OOE-12 1.25E-12 1.56E-15 8.00E-14 2.00E-14 2.57E-15 2.00E-12 5.00E-13 2.12E-14 4.00E-12 l.OOE-12
2/13/1989 2.47E-15 5.00E-12 1.25E-12 3.14E-15 B.OOE-14 2.00E-14 6.94E-16 2.00E-12 5.00E-13 2.12E-14 4.00E-12 l.OOE-12
5/15/-~ 2.50E-16 5.00E-12 1.25E-12 7.68E-15 l!.OOE-14 2.00E-14 9.03E-16 2.00E-12 5.DOE-13 8.05E-15 4,00E-12 l.OOE-12
8/14/1989 6.SOE-15 5.00E-12 1.25E-12 4.72E-15 B.OOE-14 2.00E-14 2,35E-15 2.00E-12 5.00E-13 9.95E-15 4.00E-12 l.OOE-12
11/13/1989 9.63E-15 5.00E-12 1.25E-12 4.05E-15 8.00E-14 2.00E-14 4.03E-15 2.00E-12 5.00E-13 1.99E-14 4.00E-12 l.OOE-12
2/12/1990 8.92E-15 5.00E-12 1.25E-12 3.56E-15 8.00E-14 2.00E-14 2,89E-15 2.00E-12 5.00E-13 2.69E-14 4.00E-12 l.OOE-12
5/14/1990 8.90E-15 5.00E-12 1.25E-12 3.58E-15 8.00E-14 2.00E-14 2.33E-15 2.00E-12 5.00E-13 2.09E-14 4.00E-12 l.OOE-12
8/13/1990 1.92E-15 5,00E-12 1.25E-12 1.87E-15 8.00E-14 2.00E-14 5.06E-16 2.00E-12 5.00E-13 8.86E-15 4,00E-12 1.00E-12
11/12/1990 2.91E-15 S.OOE-12 1.25E-12 2.25E-17 8.00E-14 2.00E-14 1.08E-15 2.00E-12 5.00E-13 2.19E-14 4.00E-12 l.OOE-12
2/11/1991 1.67E-16 S.OOE-12 1.25E-12 7.89E-16 8.00E-14 2.00E-14 6.38E-17 2.00E-12 S,OOE-13 4.19E-14 4.00E-12 l.OOE-12
5/13/1991 1.87E-16 5.00E-12 1.25E·12 2.61E·15 8.00E-14 2.00E-14 3.54E-16 2.00E-12 5.00E-13 1.40E-14 4.00E-12 l.OOE-12
8/12/1991 4.85E-16 5.00E-12 1.25E-12 4,38E-16 8.00E-14 2.00E-14 1.27E-16 2.00E-12 5.00E-13 2.20E-14 4.00E-12 1.00E-12
U}ll/1991 1.77E-16 5.00E-12 1.25E-12 1.46E-16 8.00E-14 2.00E-14 3.76E-17 l.OOE-12 5.00E-13 1.15E-14 4.00E-12 l.OOE-12
2/10/1992 1.83E-16 5,00E-12 1.25E-12 1.95E-15 8.00E-14 2.00E-14 l.33E-16 2.00E-12 5,00E-13 3.35E-14 4.00E-12 l.OOE-12
5/11/1992 4.40E-16 5,00E-12 1.25E-12 2.56E-16 8.00E-14 2.00E-14 4.04E-16 2.00E-12 S.OOE-13 1.41E-14 4.00E-12 l.OOE-12
8/10/1992 9.09E-17 5.00E-12 1.25E-12 1.15E-16 8.00E-14 2.00E-14 4.SOE-17 2.00E-12 6.00E-13 1.57E-14 4.00E-12 1,00E-12
_11/9/1992 2.07E-16 5.00E-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 3.62E-17 2.00E-12 S.OOE-13 2.24E-14 4.00E-12 1.00E-12
2/9/1993 1.73E-16 5.00E-12 1.25E-12 2.76E-17 8.00E-14 2.00E-14 2.89E-17 2.00E-12 S.OOE-13 3.08E-14 4.00E-12 1.00E-12
5/10/1993 2.70E-17 5.00E-12 1.25E-12 2.50E-17 8.00E-14 2.00E-14 8.74E-17 2.00E-12 S,OOE-13 1.25E-14 4.00E-12 l.OOE-12
8/10/1993 9.00E-17 5.00E-12 1.25E-12 1.76E-16 B.OOE-14 2.00E-14 O,OOE+OO 2.00E-12 5.00E-13 l.SOE-14 4.00E-12 l.OOE-12
11/8/1993 l.OOE-16 S.OOE-12 1.25E-12 l.OOE-16 B.OOE-14 2.00E-14 6.00E-17 2.00E-12 5.00E-13 1.75E-14 4.00E-12 LOOE-12
2/7/1994 1.10E-16 5.00E-12 1.25E-12 3.38E-16 B.OOE-14 2,00E-14 2.21E-16 2.00E-12 5.00E-13 3.08E-14 4.00E-12 l.OOE-12
5/9/1994 3.80E-16 5.00E-12 1.25E-12 2.82E-16 8.00E-14 2.00E-14 3.46E-16 2.00E-12 5.00E-13 1.73E-14 4.00E-12 l.OOE-12
8/9/1994 3.85E-16 S.OOE-12 1.25E-12 3.53E-16 8,00E-14 2.00E-14 1,00E-16 2.00E-12 S.OOE-13 1.00E-16 4.00E-12 l.OOE-12
lJ./7/1994 5.21E-17 5.00E-12 1.25E-12 9.70E-17 8.00E-14 2.00E-14 1.96E-16 2.00E-12 5.00E-13 1.00E-16 4.00E-12 l.OOE-12 -·-
pate Effluent Concentration Limit= 9E-14 uCi/ml BHV-4U Effluent Concentration Limit= 2E-14 uCi/ml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB
ALARA Goal= 2.25E-14 uCi/ml ALARA Goal= SE-13 uCi/ml ,ALARA Goal = 2.25E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml
Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC Limit= SE-14 uCi/ml Prel994 MPO Umlt.= 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml
Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL-SE-13 uCi/ml Pre 1994 A LARA GOAL= 1E-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
2/7/1995 3.70E-16 9.00E-14 2.25E-14 .9.80E-17 2.00E-14 5.00E-15 9.70E-17 .9.00E-13 2.25E-13 8.84E-15 G.OOE-13 1.SOE-13
5/9/1995 9.40E-17 9.00E-14 2.25E-14 2.86E-16 l.OOE-14 5.00E-15 1.90E-16 9.00E-13 z.i:sE-13 2.90E-15 6.00E-13 1.SOE-13
8/fJ/1995 1.45E-16 9.00E-14 2.25E-14 2.31E-15 2.00E-14 5.00E-15 7.10E-17 S.OOE-.13 2.25E-13 2.70E-15 6.00E-13 1.50E-13
11/11/1995 1.43E-14 9.00E-14 2.25E-14 5.70E-15 2.00E-14 5.00E-15 2.61E-15 9,00E-13 2.25E-13 5.60E-15 6.00E-13 1.50E-13
2/5/1996 1.19E-14 9.00E-14 2.25E-14 3.80E-16 2.00E-14 5.00E-15 6.10E-15 9.00E-13 2.25E-13 6.48E-15 6.00E-13 1.50E-13
5/6/1996 4.55E-16 9.00E-14 2.25E-14 3.57E-15 2.00E-14 5.00E-15 2.84E-16 9.00E·13 2.25E-13 7.68E-15 6.00E-13 1.50E-13
8/5/1996 7.78E-16 9.00E-14 2.25E-14 3.51E-15 2.00E-14 5.00E-15 1.69E-16 9.00E-13 2.25E-13 4.90E-15 6.00E-13 1.50E-13
11/6/1996 1.36E-15 S.OOE-14 2.25E-14 1.00E·16 2.00E-14 5,00E-15 4.21E-16 9.00E-13 2.25E-13 1.10E-14 6.00E-13 1.50E-13
2/6/1997 l.OOE-16 9.00E-14 2.25E-14 L40E-16 2.00E-14 5.00E-15 1.03E-16 9.00E-13 2.25E-13 6.76E-15 6.00E-13 1.50E-13
5/5/1997 l.OOE-16 9.00E-14 2.25E-14 4.00E-16 2.00E-14 5.00E-15 .2.24E-16 9.00E-13 2.25E-13 4.55E-15 6.00E-13 1.50E-13
8/11/1997 4.74E-16 9.00E-14 2.25E-14 9.07E-16 2.00E-14 5.00E-15 l,OOE-16 9.00E-13 2.25E-13 5.55E-15 6.00E-13 1.50E-13
1/5/1998 8.31E-16 9.00E-14 2.25E-14 4.82E-16 2.00E-14 5.00E-15 1.77E-16 9.00E-13 2.25E-13 5.28E-15 6.00E-13 l..SOE-13
4/28/1998 3.32E-16 9.00E-14 2.25E-14 4.43E-15 2.00E-14 S.OOE-15 1.21E-16 9.00E-13 2.25E-13 7.43E-15 6.00E-13 1.50E-13
P/31/:1998 4.60E-16 9.00E-14 2.25E-14 9.02E·16 2.00E-14 S.OOE-15 3.54E-16 9.00E-13 2.25E-13 6.91E-15 1/.00E-13 1.50E-13
9/28/1998 4.08E-16 9.00E-14 2.25E-14 4.93E-16 2,00E-14 5.00E-15 2.53E-16 9.00E·13 2.25E-13 4.52E-15 6.00E-13 1.50E-13
12/28/1998 7.72E-16 9.00E-14 2.25E-14 3.75E·16 2.00E-14 l.i.OOE-15 3.43E-16 S.OOE-13 ;1.25E-13 6.73E-15 6.00E-13 1.50E-13
3/29/1999 5.11E-16 9.00E-14 2.25E-14 4,70E-16 2.00E-14 S.OOE-15 3.70E-16 9.00E-13 ~.25E-13 8.96E-15 6.00E-13 1.50E-13
7/3/1999 5.90E-16 9.00E-14 2.25E-14 9.89E-16 2.00E-14 5,00E-15 1.28E-16 9.00E-13 2.25E-13 6.40E-15 6.00E-13 1,50E-13
9127/1999 1.70E-15 9.00E-14 2.25E-14 '7.50E-16 2.00E-14 5.00E-15 4.61E-16 9.00E·13 2.25E-13 7.86E-15 E.OOE-13 1.50E-13
12128/1999 1.03E-15 9.00E-14 2.25E-14 7.50E·16 2.00E-14 5.00E-15 2.43E-16 9.00E-13 2.25E-13 6.42E-15 p.OOE-13 1.50E-13
3/27/2000 1.00E-16 9.00E-14 2.25E-14 2.13E-16 2.00E-14 5.00E-15 2.20E-16 9.00E-13 2.25E-13 5.61E-15 6.00E-13 1.50E-13
6/2.&/1000 1.75E-16 9.00E-14 2.25E-14 .3.08E-16 2.00E-14 5.00E-15 1.11E-16 9.00E-13 2.25E-13 3.92E-15 6.00E-13 1.50E-13
9/26/2000 3.65E-16 9.00E-14 ~.25E-14 2.01E-16 2.00E-14 5.00E-15 2.24E-16 9,00E-13 2.25E-13 7.79E-15 6.00E-13 1.50E-13
12/26/2000 227E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 4.35E-16 9,00E-13 2.25E-13 8.45E-15 6.00E-13 1.50E-13
3/26/2001 1.45E-16 ~.OOE-14 .2.25E-14 l.OOE-16 ~.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.37E-15 6.00E-13 1.50E-13
7/2/2001 l.OOE-16 9.00E-14 2.25E-14 1.05E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2,25E-13 6.99E-15 6.00E-13 1.50E-13
9/24/2001 1.91E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 2.01E-16 9.00E-13 2.25E-13 8.04E-15 6.00E-13 1.50E-13
12/31/2001 1.38E-16 9.00E-14 2.2SE-14 2.05E-16 2.00E-14 5.00E·15 1.00E-16 9.00E-13 2.25E-13 1.83E-15 6.00E-13 1.50E-13
411/2002 2.20E-16 9.00E-14 2.25E-14 3.38E-16 2.00E-14 5.00E-15 1.26E-16 9.00E-13 2.25E-13 7.48E-15 6.00E-13 1.50E-13
7/l/2002 1.97E-16 9.00E-14 2.25E-14 4.10E-16 2.00E-14 5,00E-15 l.OOE-16 9.00E·13 2.25E-13 7.40E-15 6.00E-13 1.50E-13
9/30/2002 2.30E-16 9.00E-14 2.25E-14 2.42E-16 2.00E-14 S.OOE-15 1.56E-16 9.00E·13 2.25E-13 4.21E-15 6.00E-13 1.50E-13
12/30/2002 l.OOE-16 9.00E-14 2.25E-14 1.92E·16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 9.42E-15 6.00E-13 1.50E-13
B/31/2003 2.SOE-16 9.00E-14 2.25E-14 1.69E-16 MOE-14 5.00E-15 1.29E-16 9.00E·13 2,25E-13 4.55E-15 6.00E-13 1.50E-13
p/30/2003 1.00E-16 9.00E-14 2.25E-14 2.87E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E·13 2.25E-13 4.20E-15 6.00E-13 1.50E-13
9/29/2003 l.OOE-16 9.00E-14 2.25E-14 8,53E-16 2.00E-14 S.OOE-15 '3.32E-16 9.00E-13 2.25E-13 8.69E-15 6.00E-13 1.50E-13
U/'1.9/2003 1.02E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 1.49E-15 9.00E-13 2.25E-13 9ASE-15 6.00E-13 1.50E-13
3/29/2004 l.OOE-16 9.00E-14 2.25E-14 1.26E-16 2.00E-14 5.00E-15 l.OOE-16 \l.OOE-13 2.25E-13 l.OOE-15 6.00E-13 1.SOE-13
6/27/2004 1.00E-16 9.00E-14 2.25E-14 2.53E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 3.23E-15 6.00E-13 1.50E-13
9/27/2004 1.00E-16 9.00E-14 2.25E-14 l.lSE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E·13 2,25E-13 9.68E-15 6.00E-13 1.50E-13
12/27/2004 1.00E-16 9.00E-14 2.25E-14 2.30E·16 2.00E-14 5.00E-15 LOOE-16 9.00E-13 2.25E-13 1.37E-14 6.00E-13 1.50E-13
3/28/2005 l.OOE-16 9.00E-14 2.25E-14 .2.66E-16 2.00E-14 ~.OOE-15 3.15E-16 9.00E-13 2.25E-13 9.22E-15 6.00E-13 1.50E-13
6/29/2005 1.47E-16 9.00E-14 2.25E-14 1.45E-15 2.00E-14 5.00E-15 1.42E-16 9.00E-13 2.25E-13 !L34E-15 6.00E-13 1,50E-13
9/26/2005 2.01E-16 9.00E-14 .2.25E-14 2.06E-16 2.00E-14 S.OOE-15 4.80E-16 9.00E-13 2.25E-13 .2.12E-14 6.00E-13 1.SOE-13
)./3/2006 4.54E-16 9.00E-14 2.25E-14 1.24E-16 .l.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 ~.60E-14 6.00E-13 1.50E-13
4/3/2006 1.99E-16 9.00E-14 .2.25E-14 1.32E·16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.36E-15 6.00E-13 1.50E-13
7/3/2006 2.76E-16 9.00E-14 2.25E-14 2.63E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.03E-14 6.00E-13 1.50E-13
10}2/2006 4.97E-16 9.00E-14 2.25E-14 2.37E-16 2.00E-14 5.00E-15 1.00E-16 9.00E·13 2.25E-13 1.60E-14 6.00E-13 1.50E-13
1/1/2007 6.46E-16 9.00E-14 2.25E-14 2.81E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 2.10E-14 6,00E-13 l.SOE-13
4/2/2007 7.08E-16 9.00E-14 2.25E-14 3.20E-16 2.00E-14 5.00E-15 1.00E-16 9.00E·13 2,25E-13 1,54E-14 6.00E-13 1.50E-13
7/2/2007 9.41E-16 9.00E-14 2.25E-14 1.46E·l6 2.00E-14 S.OOE-15 1.99E-16 9.00E·13 2.25E-13 2.56E-14 6.00E-13 l.SOE-13
9/30/2007 3.30E-16 9.00E-14 2.25E-14 5.50E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.57E-l5 6,00E-13 1.50E-13
12/31/2007 1.42 E-15 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 9.93E-15 6cOOE-13 1.50E-13
3/31/2008 1.25E-16 !l.OOE-14 2.25E-14 7.72E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 4,09E-15 6.00E-13 1.50E-13
6/30/2008 1.28E-15 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 3.61E-16 9.00E-13 2.25E-13 1.18E-14 6.00E-13 1.SOE-13
Date Effluenl Concentration Limit= 9E-1411Cl/ml IIHV-4U Effluent Concentration Limit-ZE-14 uCi/ml BHV-4T Effluent Concentration Limit= 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml iiHV-4PB 1
A\.li!IAGoal = 2,2.51:.-'!-4 uCi/ml ALARA Goal= SE-13 uCi/ml ALARA Goal-2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uO/ml I Pre 1994 MPC Limit-SE·UuCj/ml Pre 1994 MPC Limit = BE-14 uCi/ml Pre 1994 MPC Limit= 2E-l2 uCi/ml Pre 1994 MPC Limit-llt;-12 uCI/ml I
~ 1994 ALARA GOAL= 1.25£-12 u<;!/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL= 1E-l2 uCi/iitl
Cone EFC EFCA Cone EFC EFCA Cone EFC ~FCA Cone EFC EFCA
9/30/2008 2.72E-15 9.00E-14 2.25E-14 1.27E-15 2.00E-14 S.OOE-15 7.66E-16 9.00E-13 2.25E-13 l.lOE-14 6.00£-13 1.50E-13 I
12/31/2008 2.88E-15 9.00E-14 2.25E·14 l .lOE-15 2.001:-14 S.OOE-15 6.56E•l6 9,00~13 2.2SE·13 .l38E-14 6.00E·13 1.50E-13 i
3/15/2009 1.56E-15 9.00E-14 2.25E·14 4.57E·16 2.00E-14 5.00E-15 2.99E-16 9.00E-13 2.25E-13 4.97E-15 p.OOE-13 1.50E-13
6/15/2009 5.67E-17 9.00E-14 ~.2SE·l4 2..17E-16 2.00E·M S.OOE-iS' 1.51E-16 !)_.()jiE-1~ 2..2SE·13 4.47E-15 6.00E·13 1.50E-13 '
9/15/WJ9 <tOS£-15 9.00E-14 2.25E-14 1.45E-15 2.00E-14 5.00E-15 2.52E-16 9.00E-13 2.25E-13 1.24E-14 G.OOE-13 1.50E-13
l2/iS/Z009 6,50fi-~ 9.00E-14 2.25E·14 3.48E-16 2.00E-14 5.00E-15 1.33E-16 9.00E·13 2.25E-13 7.60E-15 6.00E·l3 1.50E-13
~/3112010 6,01E-~ 9,00E-14 2.25E-14 1.26E-16 2.00E-14 5.00E-15 1.34E-16 9.00E-13 2.25E-13 :L19i-ld 6.00E-13 1.50E-13
6/S0/2010 2.3le-15 9.00E-14 2.25E-14 7.29E-16 2.00E-14 5.00E-15 2.66E-16 9.00E·13 2.25E-13 3,27E-15 6.00E-13 1.50E-13
9/30/201{) 4.ne-15 9.00E-14 2.25E·14 1.80E-15 2.00E-14 5.00E-15 S.23E-16 9.00E·13 2.25E-13 S.llE-15 &,OCE-13 1.50E-13
12/:ti-/2010 3.93E-15 9.00E-14 .2.25E·14 3.90E-16 2.00E-14 5.00E-15 2.56E-16 9.00E·13 2.25E-13 1.13E-14 6.00E·13 1.50E-13
4/4/2011 1.29E-15 9.00£-14 2.25E-14 1.40E-16 2.00E-14 5,00E·15 1.58E-16 9.00E·13 2-25E-13 l.llE-14 6,001;-13 1.5()~·13 I
7/4/?.0ll 3.30\t-15 9.00E-14 2.25E-14 5.44E-16 2.00E-14 5.00E-15 4.18E·16 9.00E·13 2.25E-13 8..26E-l5. 6.00£"13 l.'SOE-13
l013/20U 1.32£·15 9.00E-14 2.25E·14 7.89E-16 2.00E-14 5.00E-15 1.28E-16 9.00E-13 2.25E-13 1.18E-14 6JJOE-U 1.50E-13
l/3/20~2 l.04E-15 9.00E-14 2.25E·14 3.25E-16 2.00E-14 S,OOE-15 2.28E-16 9.00E·13 2.25E-13 1.14E·14 6.00E·13 1,50E-13
.4/3!20U 2.5.1E·lS 9.00E-14 2.25E-14 5.02E-16 2,00E-14 li.OOE-15 2.27E-16 I:J.OOE-13 2.25E-13 L03E•1•1 6.00E-13 1.50E-13 ,
7/2/2012 2,62E·lS 9.00E-14 2.25E·14 1.23E-15 2.00E-14 S.OOE-15 2.97E-16 9.00E-13 2.25E-13 9.27E-15 G.OOE-13 1.50E-13 I
10/1/2012 11.05<·15· 9.00E-14 .2.25E·14 8.33E-16 2.00E-14 S.OOE-15 5.43E-16 '9.00E-13 2.25E-13 1.2lE-lll s:ooE-13 1.50E-13
12/31/2012 2.32E-15 9.00E-14 2.25E-14 5,89E-16 2.00E-14 S.OOE-15 3.75E·16 9.00E·13 2.25E-13 1.56E-14 li.OOE-13 1.50!-13
3/2.5{2013 3.o.IE·l5 9.00E-14 2.25E-14 4.99E-16 2.00E-14 5.00E-15 2.79E·16 9.00E-13 2.25E-13 2.13E-14 6.00£.13 l.SOE-13
7/2/2013 :!.SOE-15' 9.00E-14 2.25E·14 3.62E-16 2.00E-14 5.00E-15 2.40E-16 9.00E-13 2.25E-13 ~.93E-15 6,00E-I.~ .L.SO~l3
•;motzoB l.98E-1S 9.00E-14 2.25E·14 4.49E-16 2.00E-14 S.OOE-15 1.54E-16 9.00E·13 2.25E-13 7.49E-15 6.00E-13 l.SOE-13
12/30/2013 3.88E-15 9.00E-14 2.25E-14 1.03E-16 2.00E-14 S.OOE-15 4.47E-17 :;J.OOE-13 2.25E-13 2.93E·14 6,00E·13 1.50E-13
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TABS
BHV-5 AIR SAMPLING GRAPHS AND DATA TABLE
Pate Effluent Concentration Limit = 9E-14 uCi/ml BHV·SU E'fRuent Concentration Limit = 2E-14 uCi/ml BHV·ST tinuent Concentration Limit-9E-13 \ICI/ml BHV-·Sft Effluent Concentration Limit-6E-13 uCi/ml BHV-SPB
AUIRAGoal= 2.~5£-14 uCI/!n! ALAAA Goal= SE-13 uCi/ml MARA Goal = 2.25£:13 uO/ml AlA_RA Goal = 1.SH311Ci/ml
Pre 1994 MPC Limit= SE-12 uCi/ml Pr" 1994 MPC limit= IIE-14 uCi/ml Pre 1994 MPC Limit= 2E·UuG/ml Pre 1994 MPC Limit = 4£'-U UCi/ml
Pre 1994 ALARA GOAL -l.lsE·lluCVml Pre 1994 ALARA GOAL = SE-13 uO(ml· Pre 1994 ALARA GOAL= lE-12 uCI/ml
Cone EFC EFCA (One EFC EFCA Cone EFC EFCA Cone EFC £FCA
9[28/1.981 ZA4E-15 S.OOE-12 1.25E-12 1.53E-15 B.OOE-14 2.00E-14 T.54E-16 2.00E-12 5.00E-13 1.69E-14 4.00£-12 l.OOE-12
12/14/1981 4.8JIM.S 5.00E-12 1.25E-12 2.78E-15 B.OOE-14 2,0tl'E-14 1.84E-15 2.00£-.H· S.OOE-13 1.53E-14 4:00E-12 1.00E-12
3/29/1982 1.04E-15 5.00E-12 1.25E-12 2.62E-15 8.00E-14 2.00E-14 l.llE-15 2.00E·ll !;.OOE-13 2.98£·14. 4.00E-12 1.00E-12
G/30/1982 3;61£,.15 5.00E-12 1.25E-12 7.EilE·l5 B.OOE-14 2.00E-14 U 9E·l5 2.00f-12 S.OOE-13 l.BOE-15 4.00E-12 l.OOE-12
9/27/1982 1.71E-14 5.00E-12 l.25E-12 9.46E-15 B.OOE-14 2.~14 3.80E-15 2.00E-12 S.OOE-13 2.35E·14 4.ooe-n l.OOE-12
l/3/191B 1.90E-14 5.00E-12 1.25E-12 5.77E-15 S.OOE-14 2.00E·l4 9.34E-17 2.00E-12 S.OOE-13 4,32£-14 4.00E-12 l.OOE-12
4/4/1983 S.OOE-12 1.25E-12 2.33E-15 B.OOE-14 2.00E-14 5.93E-16 2.00E-12 5.00E-13 3.01E-14 4.00<·12 l.OOE-12
6/30/1983 7.62E-16 S.OOE·U 1.25E-12 3.25E-15 S.OOE-14 2.00E-14 6.28E-15 2.00E-12 5.00E-13 2.69E-14 4.00t·l2 l.OOE-12
10/3/1983 4.86!'-16 S.OOE-12 1.25E-12 1.10E-15 8.00E-14 2,00E-14 3.63E-16 2.00E-12 5.00E-13 2.08E-14 4.QGE·U l.OOE>ll
l/3/<1!184 6.96£-15 S.OOE-12 1.25E-12 9.69E-16 8.00E-14 2.00E-14 9.60E-16 2.00E-12 5.00E-13 1.83E-14 4.00£·12 l.OOE·U
4~/1984 1.G41'·15 5.00E-12 1.25E-12 1.34E-15 8.00E-14 2.00E-14 3.88E-15 LOOE-12 S.OOE-13 4,Ei7E·l4 4.00E·l2 1.00E-12
7/Ul984 •l.U E-15 5.00E-12 1.25E-12 1.92E-15 B.OOE-14 2.00E-14' 3.31E-15 Z.OOE-12 S.OOE-13 2.21£-14 4.00E-12 l.OOE-12
10/l/1984 1.11E-15 S.OOE-12 L25E-12 3.13E-16 8.00E-14 2.00E-14 4.21E-16 2.00E-12 s.OOE-13 1.57&14 4.00fi-U l.OOE-12
l/2/J.985 7.32E-16 l>.OOE-12 L25E-12 6.71E-16 B.OOE-14 2.00E-14 4.94£-l li 2.00E-12 S.OOE-13 2.42E-14 4.00E-12 l .OOE-12
4n/198S 2.36E-16 S.OOE-12 1.25E-12 5.43E-16 S.OOE·l4 2.00E-14 2.71E-16 2.00E-12 S.OOE-13 1.25E-14 '4.00E-~ l.OOE-12
7/l/I!JSS 7.58E-16 S.OOE-12 1.25E-12 4.00E-16 8.00E-14 2.00E-14 6.90E-16 2.00E-12 S.OOE-13 2.15E-14 4-00E-ll l.OOE.-1.2
9/30/~985 '7 .47E-15 S.OOE-12 1.25E-12 1.16E-15 8.00E-14 2.00E-14 2.19E-15 2.00E-12 S.OOE-13 9.~0£:.15 4.00£-12 l .OOE·U
l/2/i~S6 ~ 75E-14 5.00E·l2 1.25E-12 7.24E-15 B.OOE-14 2.00E-14 3.83E-15 2.,00E-12 5.00E-13 1.13E-16 ~.00£'-U 1.00E·l'l
4(1/1986 2-m-14 S.OOE-12 1.25E-12 7.64E-15 B.OOE-14 2.00E-14 l.S1E-14 2.00E-12 5.00E-13 2.22E-14 4.00E-12 l.OOE-12
6/30/1986 2.23£.14 S.OOE-12 1.25E-12 5.19E-15 B.OOE-14 l .OOE-14 l.OSE-14 2.00E-12 S.OOE-13 2.16E-14 4.0!-TE·U 1.00E-12
10/17/1986 2.3JE--l-1 S.OOE-12 1.25E-12 7.78E-15 S.OOE-14 2.00E-14 1.60E-14 2.00E-12 S.OOE-13 2.02E-14 4.00E-12 1.00E-12
11./15/1985 [3AOE.-~4 S.OOE-12 1.25E-12 5.35E-15 8.00E-14 2.00E-14 1.47E-14 2.00E-12 S.OOE-13 2.82E-14 4.00.£..12. l.OOE-12
?1/16/1987 2.06E-14 5.00E-12 1.25E-12 4.50E-15 B.OOE-14 2.00E-14 6.74E-15 2.00E-12 S.OOE-13 7.29E-14 4.00£·12 1.00E-12
S/11/l987 2.50E-14 S.OOE-12 1.25E-12 8.54E-15 8.00E-14 2.00E-14 8.15E-15 2.00E-12 S.OOE-13 3.28E-14 4.00E-12 l.OOE-12
9/9/)Y;I 2.65E-14 S.OOE-12 1.25E-12 6.62E-15 B.OOE-14 2,00E-14 9.34E-15 2.00E-12 S.OOE-13 2.77E-14 4.00E-12 1-.00E'·U
U/2/1987 1..80E·~4 S.OOE-12 1.25E-12 7.09E-15 8.00E-14 2.00E-14 7.20E-15 2.00E-12 S.OOE-13 1.77E-14 4.00E-12 .t.oot-u
2/16/i9118 l.Ol E'lA 5.00E-12 1.25E-12 2.98E-15 8.00E-14 2.00E-14 3.93E-15 2.00E-12 5.00E-13 3.36E-14 4.00£<12 l .OOE·U
5/18/1988 1.78E-14 S.OOE-12 1.25E-12 8.14E-15 8,00E-14 2.00E-14 7.43E-15 2.00E-12 S.OOE-13 2.12E-14 4.b0e-i2 1-!IQE-12
8/15/1988 1.7.9&14 S.OOE·U 1.25E-12 1.49E-14 S.OOE-14 2.00E-14 5.34E-15 2.00E-12 5.00E-13 2.45E-14 a.oac.u 1.00E-12
Il}l~/1988 4,~6E-14 5.00E-12 1.25E-12 1.39E-14 S.OOE-14 2.00E-14 1.17E-14 2.00E-12 S.OOE-13 3.43E-14 4.00E-12 1.00E-12
2/13/198.9 1.67E-14 5.00E-12 1.25E-12 5.54E-15 S.OOE-14 r aoE-14 7.20E-15 2.00E-12 5.00E-13 5.02E-14 4.00E-12 1,00E-12
5/15/1989 2.03E-14 5.00E-12 1.25E-12 ?.OSE-15 S.OOE-14 2.00E-14 9.56E-16 2.00E-12 S.OOE-13 1.43E-14 4.00£-12 1.00E-12
S/14/').9S9 2.81E-15 S.OOE-1:2 1.25E-12 3.78E-15 S.OOE-14 2.00E-14 9.26E-15 2.00E-12 S.OOE-13 l.SOE-14 4.00E-12 l.OOE-.12
ll/13/19a!l 5.38E-14 S.OOE-12 1.25E-12 8.01E-15 S.OOE-14 2.00E-14 1.81E-14 2.00E-12 S,OOE-13 4.09E-14 4.00E-12 1.00E-12
2/12/!990 4.48E·l4 S.OOE-12 1.25E-12 1.48E-14 S.OOE-14 2.00E-14 1.28E-14 2.00E-12 S.OOE-13 3.88E-14 4.00E-12 l.OOE-12
S/14/1990 2.18E-14 S.OOE-12 1.25E-12 1.70E-14 B.OOE-14 2.00E-14 1.59E-14 2.00E-12 5,00E-13 3.49E-14 4.00E·l2 l.OOE'l~
8{13/.1990 9.5'3E,-15 S".ClOE-12 1.25E-12 1.70E-14 B.OOE-14 2.00E-14 3.27E-15 2.00E-12 5.00E-13 1.27E-14 4.00E-l2 l.OOE-12
U/12/1990 l.llE-14 5.00£·12 1.25E-12 5.27E-15 B.OOE-14 2.00E-14 5.38E-15 2.00E-12 S.OOE-13 1.56E-14 4.00E-12 1.00E-12
2/·11/1991 6.3SE·l6 5.00E-12 1.25E-12 3.13E-16 B,OOE-14 2.00E-14 2.31E-16 2.00E-12 S.OOE-13 3.89E-14 4.00E-12 l.OOE-12
5/13/1.991. 1.22E-15 5.00E-12 1.25E-12 6.14E-15 8.00E-14 2.00E-14 4.41E-15 2.00E-12 S.OOE-13 2.50E-14 4.00E-12 1,00E-12
8/12/J991 7.84E-16 5.00E-12 1.25E-12 1.43E-15 S.OOE-14 2.00E-14 4.47E-16 2.00E-12 S.OOE-13 1.84E-14 4.00£.,.:12 l.OOE-12
ll/ll/1991 5.37E-16 S.OOE-12 1.25E-12 4.20E-16 8.00E-14 2.00E-14 1.37E-16 2.00E-12 S.OOE-13 1.27E-14 4.()Qf-12 l.OOE-1'2
2/10/1992 3.54E-16 S.OOE-12 L25E-12 1.18E-16 8.00E-14 2.00E-14 4.08E-17 2.00E-12 S.OOE-13 3,69E-14 4.00E-12 l.OOE-12
5/1'1/'1.992. 4.71E-16 5.00E-12 1.25E-12 9.58E-16 S.OOE-14 2.00E-14 8.31E-17 2.00E-12 S.OOE-13 1.43E-14 4.00E-12 1.ooe:u
8/10il992 5.3:!£-15 S.OOE-12 1.25E-12 3.36E-16 S.OOE-14 2.00E-14 1.65E-16 2.00E-12 5.00E-13 1.59E-14 4.00E·l2 l.OOE'-U
11/9/1991 3.66'E-16 S.OOE-12 1.25E-12 2.25E-16 B.OOE-14 2.00E-14 l.OSE-16 2.00E-12 S.OOE-13 2.24E-14 4.00E-12 l.OOE-12
2/9/199~ 2.0JiE..l6 S.OOE-12 1.25E-12 9.14E-17 B.OOE-14 2.00E-14 6.31E-17 2.00E-12 5.00E-13 3.41E·l4 4.00E-12 l.OOE-12
5/10/1993 4.80£-16 S.OOE-12 1.25E-12 8.25E-16 S.OOE-14 2.00E-14 1.26E-15 2.00E-12 5.00E-13 l.83E·14 4.00E-12 1.00E-12
8/10/1993' l!.30.E·15 5.00E-12 1.25E-12 1.90£-16' 8.00E-14 2.00E-14 2.10E-16 2.00E-12 S.OOE-13 1.70E-14 4.00£-12 l.OOE-12
11/8/1993 2.70E-16 S.OOE-12 1.25E-12 8.00E·l7 B,OOE-14 2.00E-14 ?,OOE-17 2.00E-12 S.OOE-13 2.34E-14 4.00E-ll 1.00E-12
2/1{199~ 3.18E-16 s.oc~.-1-1 1.25E-12 l.OOE-.16 S.OOE-14 2 . .00E-14 5.18E-16 MOE-12 S.OOE-13 a.64E-14 4.001'.-12 UlOI'.-12
S/9{1994 .l.SOE·l5 S.COE·U 1.25E-12 9.78E-16 S.OOE-14 2.00E-14 1,10E-15 2.00E-12 S.OOE-13 8.30E.-15 4-00E-12 l.POE·l2
8/9/d994 2 .. 67£-15 5.006-U 1.25E-12 1.11E-15 &.OOE-1~ 2.00E-14 4.95E-16 2.00E-12 5.00E-13 l.OOE-16 4.00~-u l.D0£·12
11/1/199~ 9.lli·17 5.00E·:l2 1.25E-12 1.59E-15 I!.Q9E-14 2.00E-14 .1,66!:-l.S 2.00E-12 S.OOE-13 l.OOE-16 4.00<:·1.2 1.00E-12
D.at~ Effluent Concentration Limit= 9E-14 uCi/ml BHV·SU Effluent Concentration Limit= ZE-14 uCi/ml BHV-ST Effluent Concentration Limit -9E-13 uCi/ml BHV·SR Effluent Concentration Limit-I>E-13 uCi/ml BHV-SPB
ALARA Goal= 2.25E·14 uCi/ml ~lARA Goal= SE-13 uC[/ml ALARAGoal = Z.ZSE-13 uCi/ml ALARAGoal = l.SE-13 uCi/ml
Pre 1994 MPC Umlt -SE-12 uCi/ml Pr1> 1994 MPC Limit.: SE-14 uCi/ml Pre 1994 MPC Limit= 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml
Pre 1994 ALARA GOAL= L.25E-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 A lARA GOAL= lE-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
2/7/1995 1.51E-15 9.00E-14 2.25E-14 9.50E-16 2.00E-14 5.00E-15 9.70E-17 9.00E-13 2.25E-13 9.35E-15 6.00E-13 L50E-13
S/9/lS95 2.2rE-16 9.00E-14 2.25E-14 8.56E-16 2.00E·14 5.00E-15 3.06E-15 9.00E-13 2.25E-13 4.34E-15 6.00E.-13 l..SOE-13
8/9/199.5 1.66E-16 9.00E-14 2.25E-14 1.67E-15 2.00E-14 5.00E-15 3.90E-15 9.00E-13 2.25E-13 5.60E-15 G.OOE-13 1.50E-13
11/11/1995 2.04E-14 9.00E-14 2.25E-14 6,70E-15 Z.OOE-14 5,00E-15 7.65E-15 9.00E-13 2.25E-13 4.47E-15 6.00E-13 1.50E-13
2/5/lS<iG /1.50E-14 9.00E-14 2.25E-14 3.58E-14 2.00E-14 S.OOE-15 2.39E-14 9.00E-13 USE-13 7.30E-15 G.OOE-13 1.50E-13
S{6/l!J96 1.76E-15 9.00E-14 2.25E-14 3.57E-15 2.00E-14 5.00E-15 9.55E-16 9.00E-13 2.25E-13 7.54E-15 G.OOE-13 1.50E-13
S/S/lS'J6 2.37E-15 9.00E-14 2.25E-14 8.18E-15 2.00E·14 S.OOE-15 7.46E-16 9.00E-13 2.25E-13 S.75E-15 6.00E-13 1.50E-13
UJG/1996 3.53E-15 9.00E-14 1.25E-14 5.31E-15 2.00E-14 5.00E-15 9.39E-16 9.00E-13 2.25E-13 1.21E-14 6.00E-13 1.50E-13
2/6/iJS97 1.84E-16 9.00E-14 :2.25E-14 2.01E-16 ;2.00E-14 5.00E-15 1.87E-16 9.00E-13 2.25E-13 6.14E-15 G.OOE-13 1.50E-13
S/5/1997 5.75E-16 9.00E-14 2.25E-14 7.24E-16 .2.00E·14 5.00E-15 6.07E-16 9.om:-u 2.25E·13 4.75E-15 6.00E-13 l.SOE-13
8/11/1997 1.21E-15 9.00E-14 2.25E-14 7.39E-16 2.00E-14 5.00E-15 5.05E-16 9.00E-13 2.25E-13 4.92E-15 G.OOE-13 1.50E-13
i/'5/1998 9.89E-16 9.00E·14 2.25E-14 1.92E-15 2,00E-14 5.00E-15 6.21E-16 9.00E-13 2.25E-13 4.68E-15 6.00E-13 1.50E-13
•1{2B/J.S'J8 2.84E-15 9.00E-14 2.25E-14 2.38E-15 Z.OOE-14 5.00E-15 1.72E-15 9,00E-13 2.25E-13 7.35E-15 6.00E-13 l .50E-13
7/31/1998 7.49E-16 9.00E-14 2,25E-14 1.49E-15 2.00E-14 5.00E-15 8.34E-16 9.00E-13 2.25E-13 7.01E-15 6,00E-13 1.50E-13
9/28/1998 1.07E-15 9.00E-14 2.25E-14 9.20E-16 2.00E-14 5.00E-15 6.32E-16 9.00E-13 2.25E-13 3.95E-15 G.OOE-13 1.50E-13
12/28/1998 8.51E-15 9.00E-14 2.25E-14 4.58E-15 2.00E-14 5.00E-15 4.58E-15 9.00E-13 2.25E-13 1.43E-14 G.OOE-13 1.50E-13
3/29/1999 3.75E-15 9.00E-14 2.25E-14 2.45E-15 2.00E-14 S.OOE-15 2.39E-15 9.00E-13 :2,25E-13 B.46E-15 G.OOE-13 1.50E-13
7/3/1999 1.53E-15 9,00E-14 2.25E-14 8.65E-16 2.00E-14 5.00E-15 6.52E-16 9.00E-13 2.25E-13 7.20E-15 G.OOE-13 1.50E-13
'J/27/1999 5.83E-15 9.00E·14 2.25E-14 3.52E-15 2.00E-14 S.OOE-15 2.55E-15 9.00E-13 2.25E-13 8.22E-15 G.OOE-13 1.50E-13
12/2.8/lS'J'J 9.48E-15 9.00E-14 2.25E-14 6.20E-15 2.00E-14 5.00E-15 3.96E-15 9.00E-13 2.25E-13 7.56E-15 G.OOE-13 1.50E-13
'3{.2712TJOO 2,06E-15 9.00E-14 2.25E-14 1.27E-15 2.00E-14 5.00E-15 1.09E-15 9.00E-13 2.25E-13 7.72E-15 G.OOE-13 1.50E-13
6/26/.'1.00!l 1.50E-15 9.00E-14 l.25E-14 1.24E-15 2.00E-14 5.00E-15 1.01E-15 9.00E-13 2.25E-13 4.36E-15 6.00E-13 1.50E-13
9/'26/2000 1.04E-15 9.00E-14 2.25E-14 5.45E-16 Z.OOE-14 5.00E-15 6.01E-16 9.00E-13 2.25E-13 7.67E-15 p.OOE-13 1.50E-13
14/26/2000 1.48E-15 9.00E-14 2.25E-14 7.56E-16 2.00E-14 5.00E-15 6.84E-16 9.00E-13 2,25E-13 7,00E-15 G.OOE-13 1.50E-13
3/26/2001 4.27E-16 9.00E-14 2.25E-14 2.19E-16 2.00E-14 5.00E-15 1.89E-16 9.00E-13 2.25E-13 6.13E-15 6.00E-13 1.50E-13
7/2/2001 4.52E-16 g.OOE-14 2.25E-14 ,4.02E-16 2.00E-14 5,00E-15 1.00E-16 9.00E-13 2.25E-13 7.48E-15 G.OOE-13 1.50E-13
9/24/2001 4.65E-16 9.00E-14 2.25E-14 2.06E-16 2.00E-14 5.00E-15 2.02E-16 9.00E-13 2.25E-13 6.98E-15 G.OOE-13 1.50E-13
12/31/2001 7.40E-16 9.00E-14 2.25E-14 3.51E-16 Z.OOE-14 5.00E-15 .3.64E-16 9.00E-13 2.25E-13 4.72E-15 6.00E-13 1,50E-13
4/1/2002 1.26E-15 9.00E-14 2.25E-14 7.53E-16 Z.OOE-14 5.00E-15 7.19E-16 9.00E-13 2.25E-13 9.65E-15 6.00E-13 1.50E-13
7/1/2002 1.02E-15 9.00E-14 2.25E-14 1.03E-15 2.00E-14 S.OOE-15 3.39E-16 9.00E-13 2.25E-13 7.20E-15 6.00E-13 1.50E-13
9/30/2002 5.82E-16 9.00E-14 2.25E-14 9.28E-16 2.00E-14 5.00E-15 3.14E-16 g.OOE-13 2.25E-13 4.48E-15 6.00E-13 1.50E-13
12/;.0/200. l.OOE-16 9.00E-14 2.25E-14 7.67E-16 2,00E-14 S.OOE-15 3.48E-16 9.00E-13 2.25E-13 9.56E-15 p.OOE-13 1.50E-13
3/31/2003 1.13E-15 9.00E-14 2.25E-14 7.41E-16 2.00E-14 S.OOE-15 4.41E-16 9.00E-13 2.25E-13 6.68E-15 G.OOE-13 l.SOE-13
6/30/2003 4.35E-16 9.00E-14 2.25E-14 5.08E-16 2.00E-14 5,00E-15 2.51E-16 9.00E-13 2.25E-13 1.34E-15 G.OOE-13 1.50E-13
9/'lfJ/2003 1.51E-16 9.00E-14 2.25E-14 1.02E-16 .Z.OOE-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 7.28E-15 G.OOE-13 1.50E-13
12/29/2pa3 1.52E-16 9.00E-14 2.25E-14 1.54E-16 2.00E-14 5.00E-15 1.51E-16 9.00E-13 2.25E-13 7.02E-15 6.00E-13 1.50E-13
3/29/2004 1.00E-16 g.OOE-14 2.25E-14 1.12E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 8.82E-15 6.00E-13 1.50E-13
6/27/2004 1.18E-16 ll,OOE-14 2.25E-14 3.11E-16 2.00E-14 5.00E-15 1.25E-16 9.00E-13 2.25E-13 2.47E-15 6.00E-13 1.50E-13
9/27/2004 1.16E-16 9,00E-14 2.25E-14 1.72E-16 Z.OOE-14 5.00E-15 l.lSE-16 9.00E-13 2.25E-13 l.lOE-14 6.00E-13 1.50E-13
12/21/2004 1.14E-16 8.00E-14 2.25E-14 1.06E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 159E-14 6.00E-13 1.50E-13
3/28/2005 l.OOE-16 9.00E-14 2.25E-14 2.04E-16 2,00E-14 5.00E-15 L83E-16 9.00E-13 2.25E-13 8.57E-15 6.00E-13 1.50E-13
6/1!3/2005 1.83E-16 ·9.00E-14 2.25E-14 3.81E-16 2.00E-14 S.OOE-15 3.09E-16 9.00E-13 2.25E-13 1.06E-14 6.00E-13 1.50E-13
9/2f>{2J)GS 2.87E-16 9.00E-14 2.25E-14 8.21E-16 2.00E-14 6.00E-15 3.71E-14 9.00E-13 2.25E-13 6,28E-14 6.00E-13 1.50E-13
'l/3/2006 8.74E-16 9.00E-14 2.25E-14 3.79E-16 2.00E-14 :S.OOE-15 1.31E-16 9.00E-13 2.25E-13 4.32E-14 6.00E-13 1.50E-13
4/3/2006 5.22E-16 9.00E-14 2.25E-14 6.66E-16 2.00E-14 p.OOE-15 l.llE-16 9.00E-13 2.25E-13 !'l.34E-15 p.OOE-13 1.50E-13
7/3/200& 3.08E-16 9.00E-14 2.25E-14 1.10E-16 2.00E-14 5.00E-15 1.00E-16 8.00E-13 2.25E-13 1.25E-14 6.00E-13 1.50E-13
W/U2006 9.14E-16 9.00E-14 2.25E-14 4.95E-16 2.00E-14 S.OOE-15 1.86E-16 9.00E-13 2.25E-13 1.67E-14 6.00E-13 1.50E-13
!-/1/2007 9.49E-16 9.00E-14 2.25E-14 l>.81E-16 Z.OOE-14 S.OOE-15 2.02E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 l.SOE-13
-~/2/2007 l.OSE-15 9.00E-14 2.25E-14 8.22E-16 2.00E-14 5.00E-15 2.26E-16 9.00E-13 2.25E-13 1.64E-14 6.00E-13 1.50E-13
7/2/2007 1.54E-15 9.00E-14 2.25E-14 8.16E-16 2.00E-14 5.00E-15 4.76E-16 9.00E-13 2.25E-13 2,12E-14 6.00E-13 1.50E-13
9/30/2007 4.90E-16 9.00E-14 2,25E-14 2.37E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E·13 6.65E-15 6.00E-13 1.50E-13
12/31/2007 L46E-15 9.00E-14 2.25E-14 5.67E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.02E-14 6.00E-13 1.50E-13
3/31/2008 3.16E-16 9.00E·14 2.25E-14 6.17E-16 2.00E-14 5,00E-15 3.71E-16 9.00E-13 2.25E-13 4.82E-15 6.00E-13 1.50E-13
6/30/2008 3.13E-15 9.00E·14 2.25E-14 1.55E-15 2,00E-14 5.00E-15 9.27E-16 9.00E-13 2.25E-13 7.40E-15 6.00E-13 l1.50E-13
Date: Efllu.nf Concentration Limit = 9E-14 uCi/ml BHV·SU Effluent Concentration Limit= 2E-14 uCi/ml BHV-ST Effluent Concentration Limit-9E-13 uCi/ml ~HV-SR Effluent Concentration Limit-6E-13 uCi/ml BHV-SPB I
AI.AAA Goal = 2.25E-14uCl/~l ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml J\I.ARA Goal = 1.5E-13 uCi/mt I
Pre 1994 MPC limit= SE-12 uCi/ml Pre 1!IS4. MPC Umlt.., SE-14 uCi/ml Pre 1994 MPC Limit= ZE-12 uCi/ml pre 1994 MPC limit= 4E-12 uCi/ml
Pre 1994 ALARA GOAL-.1.25E-12 uCi/ml Pre 1994 A LARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL= lE-12 uCi/ml
Cone ~FC EFCA tone EFC EFCA Cone EFC EFCA Cone EFC EFCA
9/30l2008 7.08E-15 9.00E-14 .2.25E-14 3.41E·15 Z.OOE-14 5.00E-15 2.52E-15 9.00E-13 2.25E-13 1.15E-14 6.00E-13 1.50~-13
l'V31/200$ 7.22E·15 9.00E-14 2.25E-14 2.82E-15 2.00E·14 5.00E-15 3.03E-15 9.00E-13 2.25E-13 1.59E-14 B.OOE-13 1..50£-13
3/lS/2009 4.13E-15 9.00E-14 2.25E-14 1.39E-15 Z.OOE-14 5.00E-15 1.41E-15 9.00E-13 2.25E·13 4.66r-1S 6.00E,13 L50E-13
6/1517.00~ 2.31£,!6 9.00E-14 2,25E-14 7.79E-16 Z.OOE-14 5.00E-15 6.37E-16 9.00E-13 2.25E-13 4.18E-15 G.OOE-13 1.50E-13
9/15/2009 3.10E-l5 9.00E·14 2.25E-14 9.20E-16 Z.OOE-14 5.00E-15 6.36E-16 9.00E-13 2.25E-13 1.21E-14 6.00E·13 l.SOE-13
12/ l5/200') $.nE-ls 9.00E-14 2.25E-14 3.13E-16 Z.OOE-14 S.OOE-15 1.92E-16 9.00E-13 2.25E-13 2.48E-15 G.OOE-13 1.50E-13
3/ll/2010 4.78E--l.S 9.00E-14 2.25E-14 3.73E-16 Z.OOE-14 S.OOE-15 4.19E-16 9.00E-13 2.25E-13 1.30E-14 6,tlOE·l3 1.50E·13
6/30/UJIO 4.3SE-J.S 9.00E-14 2.25E-14 7.84E-16 2.00E-14 S.OOE-15 1.05E-15 S.OOE-13 2,25E-13 4.40E-15 G.OOE-13 1.50E·13
9/30(2010 3.57E·15 9.00E-14 2.25E-14 1.14E-15 .Z.OOE-14 S.OOE-15 7,97E-16 9.00E-13 2.25E-13 3.78E-15 G.OOE-13 1.50E·13
U/3J/2tl10 8.52E·15 S.OOE-14 2.25E-14 1.45E-15 Z.OOE-14 S.OOE-15 1.29E-15 9.00E-13 2.25E-13 1.33E-14 G.OOE-13 l.SIJE-13
4/4/20U 3,1.0E-1S 9.00E-14 2.25E-14 8.89E-16 Z.OOE-14 5.00E-15 1.10E-15 9.00E-13 2.25E-13 1.48E-14 6.00&13 L SOE·13
7/4/2011 li98E-15 9.00E-14 2.25E-14 2.03E-15 Z.OOE-14 5.00E-15 Z.SZE-15 9.00E-13 2.25E-13 l.OSE-14 G.OOE-13 J.S.0~-..13
10/3/2011 a.llE-15 9.00E-14 2.25E-14 1.14E-15 2.00E·l4 5.00E-15 5.75E-16 9.00E-13 2.25E-13 1.41E-14 li.00£,.13 l.StJE-13
l/3/UJ12 •t44E·l5 9.00E-14 2.25E·14 2.14E·l5 Z.OOE-14 5.00E-15 1.53E-15 9.00E-13 2.25E-13 Z.OSE-14 G.OOE-13 1.50E-13
4/3/2012 S.S2E·l5 9.00E-14 2.25E-14 3.24E-15 Z.OOE-14 S.OOE-15 1.79E-15 9.00E-13 2.25E-13 1.55E-14 G.OOE-13 1.50E-13
7{1./ZOU 5.87E·l5 9.00E-14 2.25E-14 3.06E-15 2.00E·14 S.OOE-15 1.21E-15 9.00E-13 .2.25E·13 l.llE-14 G.OOE-13 1.50E-13
IO/U'1,012 6.73E-15 9.00E-14 2.25E-14 2.59E-15 Z.OOE-14 5.00E-15 2.43E-15 9.00E-13 2.25E-13 1.30E-14 G.OOE-13 1.50E-13
U/31/2012 4.501:-15 9.00E-14 2.25E-14 1.62E·15 Z.OOE-14 S.OOE-15 1,79E-15 9.00E-13 2.25E-13 1.74E-14 6.00E-J.3 l.SOE-13
3/2.5/2fill 6.66E-15 9.00E-14 2.25E-14 1.48E-15 2.00E-14 S.OOE-15 l.lZE-15 9.00E-13 2.25E·13 l.SOE-14 6.00E·l3 1.50E·13
7/2(2013 7.35E·15 9.00E-14 f.25E-14 1.72E-15 2.00E·14 5.00E·15 2.02E·15 9.00E-13 2.25E-13 6.67E-15 &,OOE-13 l.SOE·l3
9/30/20)3 2..78E·15 9.00E-14 2.25E-14 6.92E-16 Z.OOE-14 5.00E-15 3.29E·l6 9.00E-13 2.25E-13 6.62E·15 6.00E·l3 1.50E·l3
12/30/2013 6.70E·15 9.00E-14 2.25E-14 3.93E-16 2.00E·14 5.00E-15 2.53E-16 9,00E-13 2.25E-13 2.78E-14 G.OOE-13 1,50E·13
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66-das
B6-das
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TAB6
BHV-6 AIR SAMPLING GRAPHS AND DATA TABLE
..
Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-6U Effluent Concentration Limit-2E-14 uCi/ml BHV-6T Effluent Concentration Limit= 9E-13 uCi/ml liHV-6R Effluent Concentration Limit= 6E-13 uCi/ml BHV-6PB I
ALARAGoal = 2.25E-14 uCi/ml ALARA Goal= SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARA Goal= ,l.SE-13 uCi/ml
I
Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit= 8E-14 uCi/ml Pre i99,41'\11PC Limit = 2E-12 uCi/ml Pr& 1994 MYC Umll ~ 4E-12 uCi/ml
Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL-SE-13 uCi/ml Pre 1994 ALARA GOAL= lE-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
9/28/1981 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
12/14/1981 S.OOE-12 1.25E-12 B..OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
3/29/1982 5.00E-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l .OOE-12
6/30/1982 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
9/77/198]. S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
1/3/1983 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00£-12 l.OOE-12
4/4/1983 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
6/30/1983 5.00E-12 1.25E-12 B.OOE-14 2.DOE-14 2.DOE-12 5.00E-13 4.00E-12 1.00E-12
10}3/1983 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.DOE-13 4.00E-12 l.OOE-12
1/3/1984 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12
4/2/1984 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
7/2/1984 5.00E-12 1.25E-12 8.00E-14 2.00E-14 z.OOE-12 S.OOE-13 4.00E-12 1.00E-12
10/1/1984 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
1/2/1985 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 A.OOE-12 1.00E-12
4/1/~9~5 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
7/-t/198'5 :S.OOE-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
9/30/1985 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
1/2/1986 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
4/1}1986 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
6/30/:1986 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
10/27/1986 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2,00E-12 S.OOE-13 4.00E-12 l.OOE-12
12/15/1986 5.00E-12 1.25E-12 S.OOE-14 2.00E-14 2,00E-12 S.OOE-13 4.00E-12 l.OOE-12
3/16/1987 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
5/11/1987 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12
9}9/1987 5.00E-12 1.25E-12 8.00E-14 2.00E-14 l.OOE-12 5.00E-13 4,00E-12 l.OOE-12
11/2/1987 5.00E-12 1.25E-12 8.00E-14 :l.OOE-14 l .OOE-12 S.OOE-13 4.00E-12 l.OOE-12
2/16/1988 S.OOE-12 1.25E-12 8.00E-14 l .OOE-14 2.00E-12 i>.OOE-13 4.00E-12 l.OOE-12
~/18/1988 5.00E-12 1.25E-12 8.00E-14 .2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12
8/15}1988 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
11/14/1988 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
2/13/1989 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
5/15/1989 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
8/14/1989 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
11/13/1989 S.OOE-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.DOE-12
2/12/1990 S.OOE-12 1.25E-12 8.00E-14 MOE-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
5/14/1990 S.OOE-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
8/13/1990 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 · 4.00E-12 1.00E-12
11/12/1990 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
2/11/1991 5.00E-12 1.25E-12 8.00E-14 2,00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
5/13/1991 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12
8/12/1991 S.OOE-12 1.25E-12 B,OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
11/11/1991 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
2/10/1992 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 .l.OOE-12 5.00E-13 4.00E-12 l.OOE-12
S/11/1992 5.00E-12 1.25E-12 8.00E-14 2.00E-14 l.OOE-12 S.OOE-13 4.00E-12 1.00E-12
8/10/1992 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
11/9/1992 S.OOE-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12
7./9/lm 5.00E-12 1.25E-12 S.OOE-14 2.QOE-14 2.00E-12 5.DOE-13 4.00E-12 1.00E-12
5/10/1993 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12
8/10/1993 5,00E-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
11/8/1993 S.OOE-12 1.25E-12 /l.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
2/7/1994 S.OOE-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
5/9/1994 S.OOE-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
am'J9(j4 5.00E-12 L25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
lJn/199il 5.00E-12 1.25E-12 B.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
031!! Etnu~nt Concentration Limit= 9E-14 uCJ/ml BHV-6U Effluent Concentration Limit= 2E-14 uCI/ml BHV-61" a nuimt Concentration Limit= 9£.13 uCl/ml 8HV·6R Effluent Concentration Limit = se-13 uCJ/mJ BHV-6PB
IUAfiAGoal = 2.25E-14 uCI/ml ,.~LARA Goal = 5E-13 1iC"1/ml AlARAGoal = 2..25£-U'uO/ml AtARAGoal = l .SE-13·uCi/ml
Pre 1994 MPC Limit= SE-12 u0 /1'111 PrB 1994 MPC Limit= 8E·l!l uCl/ml Pre 1994 MPC Limit= 2E'l2·uCi/ml Pt~ 1994 MPC Limit= 4E·l2 uertml
P~ 1994 ALARA GOAL = 1..25E-l2 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1£.!2 uCl/ml
Coru: E.FC EFCA Co~ EFC. EFCA <:one EFC EFCA Cone EFC EFCA
2/7/1995 !!.00£'-l.ol 2.25E-14 2.00E-14 S.OOE-l-5 9.00&13' 2.2SE-B 6.00E-13 1.50E-13
gg/1995 9.00E-14 2.25E-14 2.00E-14 S-OOE-15 9.00€-13 2,25E-13 6.00£-13 1.50E-13
8/9/1995 9.00€-14 2,25E.-j4 Z.OOE-lA S.(lOE-15 9.00E-B 2.25E·l3 6.00ii.-13 1.50E-13
ll/U/1995 9.00E•l4 :ust:-14 2.0QE.l.~ S.OOE·l.S 9.0j)E=l~ 1..25E-l3 G.OOE-13 l.SOE-13
'l/S/'19% 9.00E-l4 '2.25€-14 2.00!:-14 5.00E-15 9.00E-13 2.25E-13 6.006-13 1.50E·B
S/6/1996 9.'00E-14 2.25E-14 2.00E-14 S.OOE·15 9.oQE-13 2.25E·H 6.00E-13 1.50E-13
8/5/!JE96 9..00E.·.14 2.25E-14 2.00E-14 S.OOE-15 9.00E'-13 2,25E·l3 6.00£-13 1.50E-13
ll/6/1!3% 9.00E·l4 ~E-14 '2.00E·l4 5.00E·l5 9.00E-l3 2.25E-13 6.00.E•1~ 1.50E-13
1/6/1997 9.00£-14 2.2SE·l4 2.00E-14 S.OOE-15 9.00E"·l3 2.25_E-13 li.OOE-B 1.50E-13
5{5/1$7 9.PQE-l4 z.zSF-14 2.00E-14 5.00E-15 9.00E·l3 2.25E-13 6,00E·l3 t..5oe-13
l!/U/1997 9.00.E-l~ 2.25£.14 Z.OOE,-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13
1/5/1998 g.O(JE-14 2.25E-14 2.00E-14 S.O()HS 9110E.l3 :Z:25E-13 6.00E-13 1.50E-13
4/2JJ~93 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.1Xlf-13 2-lsE-13 (i'.OOE-lS 1.50E-13
7/3.l!l!J98 9~00E-l4 2.2.SE-14 MOE·14 S.I)OE-15 9.00E-.l3 2.25E=l3 G.OOE-13 1.50<-13
9/2S/t99S 9.00.E"·14 2.2SE'-lA 2.~W4 5.00E-15 9.00E·l3 2.25E-13 G.OOE"-13 i;>OE-~3
12/28/.1998 9,00E-!4 U5E·14 2.1JO~·l4 5.00E-15 9.00E-13 2.25E-13 6.0QE-l3 1.50E·13
3/'l9/1YJ9 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13
1/3/1999 9.00E-14 2.25E-14 2.00E-14 5.00£-15 9.00E-13 2.25E-13 &.00£.13 1.50E-13
9/27/1S99 3.03E-15 9.001'--14 2.2SE-l4 1.37E-l5 2.om;.J.q S.OOE-15 s.n&t!i 9.00E-13 2.25E-13 7.55E-15 6.00E-l3 1.50E-13
12/211/1999 S.OlE·lS 9.00E-!.4 2..25E·l4 2.89E-1S 2.00E·14 5.00E-15 1.31E-15 9.00E-13 2.25E-13 8.10E-15 6:00E-13 :LSOE-B
"!J/30/2000 7.46E-16 .S.OOf.14 l ,251i-14 5,2SE·1,6 l.OOE-14 5,00E-15 3.00E-16 9.00E-13 2.25E-13 7,83E-15 SOQE·i3 ~13
_6/Z6/:ZOOO 5:40E"-l6 9-00E-14 2.7..5"E·l4 3.53E-16 2.00E-14 5.00E-15 6.UE.-16 9.00E-13 2.25E-13 4.83E-15 6.00E-13 1.SOE-13
9/25/2000 3:7SE•16 9.00H4 2.isE-14 2.23E-16 2.00E-14 5.00E-15 L91E·16 9.00E-13 2.25E-13 6.41E-15 6.0QE-13 1.50E-13
12!2&/aooo 5.21E-16 9:00E--14 ~.:25E·l4 3.39£-16 2.00E·14 5.00E-15 3:28E·U 9.00E-13 2.25E-13 8.57E-15 6.00E·H 1.50E-13
3/26/2001 !.42E'-1G 9.()()E·14 z.m-14 l...OOE-16-~OOt-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.15E-15 6..00£-13 LS00;.13
712/2001 1:8lE-16 9.00E-14 z,25E·ld 1.66E-16 2,00f-14 5.00E-15 1.00E•l6 9.00E-13 2.25E-13 6.95E-15 &.OO"E-13 LSOE-13
9/2.4/2001 3.08!-16 9.00Eo1:4 2.2$-~4 1.01E-16 01,00£·14 5.00E-15 1.77E-16 9.00E-13 2.25E-13 8.59E-15 6.00E-l3 l.SOE-13
12/31/2001 3.3~E-l6 9.00E·l4 2.25E-14 1.25E-16 2.00E-14 5.00E-15 1~·16 9.00E-13 2.25E·l3 3.14E-15 6.00E-13 1.50E-13
4/I/2002 4.77E-16 9.00E-14 2.25E·14 ~41!-16 2.00E-14 5.00E-15 l..96E-16 9.00E-1'.J 2.2SE·.I3 8.61E-15 6.00E-13 1.50E-13
7/1/2002 3,68E-16 9.00E·l•1 2.2.SE·:14' 4.41E·16 2:00£-14 S.OOE-15 1 76E-16 9.00E-1~ 2.25€-13 8.20E-15 6.00E"·1~ 1.50E-13
9/a0(2002 3.67E-16 9.00t-14 2.2SE-l4 S.GOE-1.6 2.00E-14 5.00E-15 l.BOE-16 9;00E·J3 2.25E-13 5.55E-15 6_00£·13 l.50E·l3
12/SIJ/2002 1.00E-16 9.00E-14 2.2SE-14 3.43&16 2.00f·l4 5.00E-15 1.67E-16 9.00E-l3 2.25E-13 1.35E-14 6,00£-13 1..50£·13
3/3"112003· 1.98E-16 9.00£-1~ 7..25E-14 1.68E-16 Z.OOE-14 5.00E-15 l.OOf-16 9.00E-13 2.25E-13 7.77E-15 6.00E-13 1.50E-13
6/30{1003 l.lBE-16 !l.OOE-14 2,25E-14 1.15E-16 2.00E-14 s .. OQE·tS J.Oof·16 9.00E-U 2.25E·B 5.921:-15 6.00E-13 1.50E-13
9/29/2003 1.00E-16 9.00E-14 2.2SE·lll l.OOE-16 2.00E-14 5.0CE·l5 1.00E-16 9.00£·13 USE-13 S.30E-1S (i'.OOE-13 1.50E-13
~2/29/2003 1.00E-16 9.ooE-l4 2.2SE·14 1.36£·16 2..00E·14 S.OOE-15 l.OOE-16 9.00E-13 2.25£'-13 6.66E-1$ li.OOE.·13 l.SOE-13
>tz9/2004 l.OOE-16 9.00E-14 2:25<'"14 l.OOE-16 2..00E.·14 5.00E-15 l.OOE-16 9.()!la-13 2.2SE-13 8.17£.15 6.00!:-13 l.S'OE-13
6/27/2004 l.OOE-16 9.00E-1.4 2.25E·14 l.OOE-16 2;QCE-l4 5.00E·15 1.00E·16 9.00E-13 2.25E-13 3:S.5E-J.5 6.0(!E-l3 l.:;<lE·lJ
9/27/UJe4 1.00E-16 9.001:--14 2.25E-14 1.38E-16 2.00E-14 S.OOE-15 l.OOE·l6 9.00E-13 2..25£,13 1,22E.-l4 6.00E-13 1.50E-13
rl/2712004 1.05E-16 9.00E-14 2.2SE"·l~ 1.72E-16 2.00E-14 fs.DOt·l$ l.OOE-16 9.00E·U 2.25~13 1..52E-.14 6.00E-13 1.50E-13
3/28/2005 l.OOE-16 9oOOE-14 2.2.51:-14 ~.OOE-1.6 2.00E-l'l S.OOE"·15 1.00E-16 9-00E-ll 2.25£-13 9-'l'IE-15 fi.OOE-13 1.50E-13
6/i.9/')005 1.28E-16 9.00E·l4 2:2:SE·l4 l.QJE·l6 2.00£-14 5.00£-15 l .OOE-16 9.0!lE-1!1 2.25£-13 9.&5£-15 61)()&13 l..SOE·13
9/26/2005 1.98E-16 9.o::fE-M 2.25£·14 5.98£-16 ·2.QOE:-l4 5.00E·15 3.55E-16 9.00E·l3 2.25E-13 1.71E-14 G.OOE-13 l..SOE-13
1/312006 7:67E-16 9.00£·1.4 2.25E-14 2.88E-16 2.00.E-l4 5.00E-15 3.60E·l5 9.00E-13 2.25E-13 4.85E·.1.4 6.00E·lil l.SCJE'-ll
4/3/2fYJ6 2.92E•l6 MOE-14 2.25E-14 2.00E-16 2.00E-14 S.OOE-15 I.,OOE-16 9.00£-U 2.2s£-1a l.llE-14 6.00E-13 1.50E-13
7 /I3'/2IJIJ6 3.25E-16 9.00!1-111 ·2.25E-14 2.3GE-16 2.00E-14 S.OOE·lS" 1.08£-16 <J,o6E-13· 2.25"£-13 1.10E-14 6.00E-13 1.50E-13
10/2/2006 5.03E-16 9.00H4 2..2SE-14 l :49E-lo 2.0oE-i4 S.OOE.-15 U9E-16 9.00E"·l3 2.2SH3 2.13E·15 6.00£-13 1.50E-13
l/1/2007 8.31E·16 9.00E-l4 2 •. 25E-14 2.49E-l& 2.00£·1.4 5.00E-15 1.00E-16 9.00£-13 2.:25E·l3 1.70E-14 6.00£·13 LSOE·13
4/212007 5.36£-16 g.OOE·14 2:25E·14 .J.l.SE-16 2.pOE-14 S.OOE-15 1:00E·l6 9.00E-13 2.25E-13 1.43E-14 6.00E-l3 l.SOE"-13
7/2/2007 l.OBE-15 9,00E•l4 2.25E-14 2.18E-16 2.00E-14 S'.OO!r-15 1.54E-16 9.00E-13 2.25E-13 2.04E-14 6.00E-13 1.50E-13
9/3P/2007 3.92E-16 9,00E-14 2.25E-14 1,0:1:!:-15 2.00E-14 5.00&15 l.OOE-16 9.00E·13 2.25f·lA U8E-l5 6.00E-13 1.50E-13
ll/ll./2007 2.92E-15 9.00E-14 2.251:.-14 LS5E.·l5 2.0\JE-14 >.OOE-15 :UGE-.16 9.00E·B 2i2.5~-l3 9.19E-15 6,00t.-13 1.50E-13
3/31/2008 d.34£-1fi 9.001!:·1~ 2..25t·l4 HlE-lli 2.00E·l4 S.OOE-15 l.OOE-16 9,00E·l3 2.25E-U S,99E-1S 6.00£·13 1.5flE:l3
6/3102008 ..... j,88£·15 9.DO.E-l4 2.2J>E.l4 9.00£-16 -----2.00E-14 5.00E-15 4.04E-16 -9.00E·l3 2.25E-13 7.-41€-15 6.00E-l3 150E·1'3
Date E-ffluent Concentration Limit= 9E-1.4 uCi/ml BHV-6U Effluent Concentration Limit= ZE-'14 uCi/ml BHV-6T Effluent Concentration Limit = 9E-13 uC:I/ml BHV-6R Effluent Concentration limit-6£-13 uCI/."11 BI-W-6PB_I
AtARAGoal= 2.25E-14 uCi/ml ALARAGoal= SE-13 uCi/ml All\RAGoal = fusE-13 u0/"1l AlARAGoal-t.SE-13 uCi/ml ! Pre 1994 MPC Limit= SE-U·UCJ/ml Pre 1994 MPC Limit -8Eool4 tiCi]ml P~ 1994 MPC Limit= 2E-12 uCi/ml Pre 1994 MPC'Lilnlt"' 4E-12 uCi/ml
I Pre 1994 ALARA GOAL= u.sr-12 uCI/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL= :tE-12 uCi/ml
Col" ER: e:cA cOne EFC . EFCA Cone EFC EFCA Cone EFC EFCA
9/30/2008 4.82E-15 9.00£-14. 2.25E-14 2.10E-15 2.00E-14 5.00E-15 1.27E-15 9.00E-B 2.25E-13 l.llllli·14 6.00E-13 1.50E-13 ,
12/31/2008 4.80E-15 9.00E-14 2.25E-14 1.70E-15 2.00E-14 5.00E-15 1.25E-15 9.00E-13 2.25E-13 1.49E-14 6.00E-13 1.50E-13
3/15/2009 2.77E-15 9.00E·14 2.l.5E-14 1.01E-15 2.00E-14 5.00E-15 7.82E-16 9.00E-13 2.25E-13 6.46E-15 6.00E-13 1.50E-13 ·
6/15/2009 1.41E-16 9.00E'l4 2.25E-14 2.67E-16 2.00E-14 5.00E-15 1.81E-16 9.00E'13 2.25E-13 5.76E-15 6.00E-13 1.50E-13
9/15/2009 4.87C-1S 9.COE·l4 ~75E·l4 4,32£.16 2.00E-14 5.00E-15 2.23E-16 9.00E-13 2.25E-13 8.98E-15 6.00E-13 1.50E-13
12/15/2009 9.24E-15 9.00£-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.15E-16 9.00£-13 ~.2SE·l3 ~.44E·l5 6,00E-13 1.50E-13
3/3l/2010 9.63E-15 9.00E-14 2.2SE·lll 1.82E-16 2.00E-14 5.00E-15 2.06E-16 9.00E-13 2.25E-13 1.37E-14 6.00E-13 1.50E-13
6/30/2010 3.62E-15 !J".OOE-.14 2.25E-14 3.94E-16 2.00E-14 S.OOE-15 4.89E-16 9.00E-l3 2.25E-13 ~.:iOE-15 &.oot-u l-'iOE-13
9/30/2010 5Jt7~15 9.00£-14 2.25E-14 l.08E-15 2.00E-14 5.00E-15 5.68E-16 9.00E-13 2.25E-13 3.98E-15 6.00E-13 1.50E-13 I
12/31/2010 1.24E-14 9.00E-l4 2.25E-14 1.21E-15 2.00E-14 5.00E-15 1.00E-15 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13
4/4/2011 2.70E-15 9.00E·l4 2.2SE-14 C.62£·1.6 2.00£-14 S.QI)E-lS 6.51E-16 9,00E-13 2,25E-13 1.29E-14 6.00E-13 1.50E-13
7/4/2011 ~.01£-15 9.00E-14 2.25E-14 7.07E-16 2.00E-14 5.00E-15 5.75E-16 9.00E-13 2.25E-13 7.97E-15 6.00E-13 1.5m'-13
10/3/2011 2.0SE:·15 9.00E-14 2.25E-14 6.12E-16 2.00E-14 5.00E-15 1.88E-16 9.00E-13 2.25E-13 9.93E-l5 6.00E-13 1.50E-13
1/3/2012 3.14E-15 9.00E-14 2.25E-14 1.09E-15 2.00E-14 5.00E-15 7.65E-16 9.00E-13 2.25E-13 l..89C-t4 6.00E-13 1.50E-13
4/3/2012 4.41E-15 9.00E·lll Z2SE-14 1.82E-15 2.00E-14 5.00E-15 4;0QE-16 9.00E-13 2.25E-13 1.50E-14 6.00E-13 l.SOE-13
7/2/2012 6.42£-15 9.00E-14 2.25E-14 2.25E-15 2.00E-14 5.00E-15 S.llE-16 9.00E-13 2.25E-13 9.54E-15 6.00E-13 l.SOE-13
10/1/2012 6.63E-.15 9.00E-14 2.25E-14 1.31E-15 2.00E-14 5.00E-15 1.22E-15 9.00E-13 2.25E-13 1.34E-14 6.00E-13 1.50E-13
12/31/2012 3.83E-15 9,00E-'14 2.l.5t.-1A 1.18E-15 2.00E-l4 S.OOE-15 9.30E·l6 9.00E-13 2.25E-13 1.60E-14 6.00E-13 1.50E-13
3/25/2013 4.52£-1.5 9.00E-14 2.25E-14 7.93E-16 2-!),0E-14 5.00E-15 4.91E-16 9.()9E,I3 2.25E-13 1.70E-14 6.00E-13 1.50E-13
7/2/2013 5.91£-15 S.OOE-14 2.25E-14 6.74E-16 2.00E-14 5.00E-15 7.85E-16 9.00E-ll. 2.15£-13 S.lSE-15 G.OOE-13 l.SOE-13
9/30/2013 2.68E-15 9.00E-14 2.25E-14 3.97-E-16 2.00E·l4' S.OOE-15 1.04E-16 9.00E-l3 2.25E-13 6..13E-15 G:OOE-13 1.50E-13
12/30/2013 1.60E-14 9.0QF.-l4 2..25£·1.4 2.48£-16 z.ooE-14 S.I)()E-15 1.05E-16 9.UOE·13 2-ZSE-13 2.67E.-14 6.00£·13 1.50E-13
----
0 c 0 ~ "-.... c C1) u c 0
(.)
C1)
"C
u
::::J c .g
"C cu a:
CD :> :J: m
C\J ,....
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~
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-
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-
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-----
~
--
--
-. .
. -
-
----.
.
(X) ,.... w ,....
900c/08/6
SOOc/9c/6o ,....
C\J I "'0 «! Q) .....J
cOOc/08/6 +
<0 ~ E :::1 666 ~ILGI6'g
a:
+
966~/S/9 g
C\J E
:::1 ·c 0 ~ 1-
866 ~/0~/9 +
~ :::1 066~/8~/9~
E .:2 c: ~ ::>
L96~/6/6 +
t>96 ~/~/0 ~
~96 ~/9c/6
t/) c 0 ·~
lo-.... c Cl) u c 0 (.)
ca lo-
::::s -; z I E
::::s ·-c ca lo-
::J
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I I LLJ LLJ 0 0 ~ ~ .,.... .,....
~~== ~.
,.
~N ~ ~ .. ,...~
~~ ,_
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C') """ .... ....
I I w LLJ 0 0 ~ 0 .,.... (a1eos oo1)
. . --
800c/08/6
I .
~ .
~~~ -. -. ~ . 900G/9c/6 . . . -
~ .
~~ '-" . . .
""' -~ -.
cOOG/08/6
• -
666~/LG/6
.
.
. 966 ~/9/8
. 866 ~/0~/8
--.
066 ~/8~/8
-
L86~/6/6 --
. -1786 ~/~/0~
-
-.
-~86 ~/8G/6
1.{) CD ,..._ .... .... ....
I I I w LLJ LLJ
0 0 0 0 0 ~ .,.... ....
c
.€ 0
:::::1 -tn c 0 i "--c
(I) u c 0 0
0 M N I E
:::::1 ·;:
0 ~ J-
eD > ::I:
al
C\1 (') ,...... ,......
I I w w 0 0 ~ ~ ,......
• ~
~
~K
~ r.
I"""""
""'" LO ,...... ,......
I I w w 0 0 0 ~ (are:>s Bo1) ,......
~~ ~ . -.
--~ ~OG/8/0~
it -.... -
I4F:; ~ ~ , . • ----800G/08/6
~ ~ ~
~ p. -
l::f--' .
I~ 900G/9G/6
~~ ~ ~
~ N -~ . ~ ~
GOOG/08/6
666~/LG/6
.
---
966~/9/8
.
-866 ~/0~/8
~
. 066 ~/8~/8 --
-.
L86~/6/6
.
-.
1786~/~/0~ 0
-
' ~86~/8G/6
<0 I'-,...... ,......
I I w w 0 0 ~ ~ ,......
1.00E-11
1.00E-12
1.00E-13
Q) ca (.)
C!.I .OOE-14
Ol 0 :::!-
1.00E-15
1.00E-16
1.00E-17
.
T"" CX)
Ol
T"" to ~ Ol
Effluent Concentration Limit= 9E-13 uCi/ml
ALARA Goal= 2.25E-13 uCi/ml
Pre 1994 MPC Limit= 2E-12uCilml
Pre 1994 ALARA Goal= SE-13 uCilml
. • • • r r o::t CX)
Ol
T"" ......
T"" 0
T""
. ' . ' ,...._
CX)
Ol
T"" ~
0 Ol Ol
~
T"" ro
. ' ' ('I)
Ol Ol
T"" 0
T"" ro
\
' '
.
BHV-6 Radium-226 Concentrations (uCi/ml}
-------------------
CD Ol
Ol
T"" ...... 10 ro
'
~
' Ol Ol Ol
T"" -;:::
~
'
'
N\
' .
0 0 ~ ('I)
05
1
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~
T .... I_
~ 1•1
l.JJ.~ ·v
I ' I f ' I 1 I I I ~ •
0 0 ~ ~
~
v ~
v
T"" 0 ~ 0
::::::-E -0 ::::s -tn c 0 ·~
1-.... c C1) u c 0 0
0 ,....
N I "C cu j
co :> :I: c.c
T""
T""
I w 0 ~
T""
C\J Cl)
T"" T""
I I w w 0 0 ~ ~
T"" T"""
~
~
+:: ~
~
·~
_.J
Fi--~
~ ~
.::::
l:oll
•
""'" T"" I w 0 0
(areos Bol)
------
~ LOG/8/0 ~
-
900c/08/6
-.
-
. 900c/9c/6
-
> -
----cOOc/08/6 --
-666~/LC/6
-
966 ~/9/9
. 866~/0 ~/9
.
-.
066 ~/8 ~/9
.
I L86~/6/6
-
-
v96 ~~~~o~ . . . .
-.
-~86~/9G/6
LO (!) ,.....
T"" T"" T""
I I I w w w 0 0 0 ~ ~ ~
T"" T"" T""
ATTACHMENT C
BHV AIR SAMPLING LABORATORY RESULTS AND QAIQC
EI\ERGY
• : II
Helen1, MT 117-472-G711 • Billinp, MT 8GI-135-4tn • Cuper, WY 111-235-1515
Gillllb, IVY' IH-III-7115 • Rapid City, SO 111-172-1225 • Ccllep Station, IX 111-111-2211
November 11, 2013
Energy Fuels Resources (USA) Inc
225 Union Blvd Ste 600
Lakewood, CO 80228-1826
Workorder No.: C13100250
Project Name: 3rd Quarter Air 2013
ANALYTICAL SUMMARY REPORT
Energy Laboratories, Inc. Casper WY received the following 6 samples for Energy Fuels Resources (USA) Inc on 10/7/2013
for analysis. ------
Sample ID Client Sample ID Collect Date Receive Date Matrix Test
C13100250-001 BHV-1 09/30/13 00:00 1 0/07/13 Filter Composite of two or more samples
Metals, Total
Digestion, Total Metals
Lead 210
Radium 226
Thorium, Isotopic
C131 00250-002 BHV-2 09/30/13 00:00 1 0/07/13 Filter Same As Above
C131 00250-003 BHV-4 09/30/13 00:00 1 0/07/13 Filter Same As Above
C131 00250-004 BHV-5 09/30/13 00:00 1 0/07/13 Filter Same As Above
C131 00250-005 BHV-6 09/30/13 00:00 1 0/07/13 Filter Same As Above
C131 00250-006 Blank 09/30/13 00:00 1 0/07/13 Filter Same As Above
The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were
performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted.
Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601 ,
unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical
Report, the QNQC Summary Report, or the Case Narrative.
If you have any questions regarding these test results, please call.
Report Approved By:
Digitally signed by
Steve Carlston ,/(-t-f? ~
/ · Interim Branch Manager
Date: 2013.11.11 18:04:08 -07:00
Page 1 of22
EI\ERGY
' ''' . llelell1, liT 877-472-1711 • Billinp,IIT IIGI-735-4481 • Cuper, W'f III-23W515
Glllllte, W'f ........ 7175 • Rapid City, SD 118-172·1225 • Co11eae Stati011, TX IIUII-2211
CLIENT: Energy Fuels Resources (USA) Inc
Project: 3rd Quarter Air 2013
Sample Delivery Group: C13100250
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Report Date: 11/11/13
CASE NARRATIVE
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this
method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should
be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of
counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven
individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB
monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy "Lab"orarorles. Inc. -Gillette, WY
eli-h-Energy Lab.oralories, Inc.-Helena, MT
eli-r -Energy LaboratorieS, Inc. -Rapid City, SO
eli-cs -Energy Laboratories, Inc. -College Station, TX
Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College
Station, TX, EPA Number TX01520.
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA;
Oregon: WY200001 , Radiochemical WY200002; Utah: WY00002; Washington: C836
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under
these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of
origin. Please verify Ell's certification coverage by visiting www.energylab.com
Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web
page www.energylab.com.
Page 2 of 22
EI\ERGY Hlilne,MT 177-472-0711 • Billinp,MT Ill-735-4411 • Casper, WY 111-235-1515
Gillelle, WY Rl-lll-7175 • Rapid City, SD 111-172-1225 • Collele Sution, TX 111-191-2211 --...._..._
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources {USA) Inc
REPORT DATE: November 11,2013
PROJECT: 3rd Quarter Air 2013
SAMPLE ID: BHV-1
Quarter/Date Sampled Concentration
Air Volume Radionuclide 1JCilmL
ICI3040210-00I naLU 9.91E-16
Frrs~ Quarter 20 13 2JoTh 1.86E-16
Air Volume in mLs 226Ra 2.04E-16
1.36E+ll 210Pb 1.82E-14
Quarter/Date Sampled Concentration
Air Volume Radionuclide 1JCilmL
.CI3070231-00I nalu 1.46E-15
Second Quarter 20 13 2JoTh 3.34E-16
Air Volume in mLs 226Ra 3.91E-16
1.34E+ll 210Pb 5.78E-15
Quarter/Date Sampled Concentration Radionuclide Air Volume I!CilmL
c 13100250-00 1 ""U 8.89E-16
Third Quarter 20 13 23oTh 9.13E-17
Air Volume in mLs 226Ra 1.05E-16
1.37E+ll 210Pb S.OOE-15
+LLD's are from Reg. Guide 4.14
Counting
Precision
1JCilmL
N/A
5E-17
IE-17
2E-16
Counting
Precision
,..ci/mL
N/A
SE-17
2E-17
IE-16
Counting
Precision
1JCilmL
N/A
3E-17
IE-17
1E-16
*Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDC 1JCilmL
N/A
2E-17
4E-18
5E-17
MDC I!CilmL
N/A
2E-17
3E-18
6E-17
MDC 1JCilmL
N/A
2E-17
2E-18
4E-17
L.L.D.+ Effluent Cone.* %Effluent
,..cilmL ,..cilmL Concentration
1E-16 9E-14 l.IOE+OO
IE-16 3E-14 6.21E-01
IE-16 9E-13 2.27E-02
2E-15 6E-13 3.03E+00
L.L.D.+ Effluent Cone.* %Effluent
1JCilmL 1JCilmL Concentration
IE-16 9E-14 1.62E+00
IE-16 3E-14 l.llE+OO
lE-16 9E-13 4.35E-02
2E-15 6E-13 9.64E-01
L.L.D.• Effluent Cone.* % Eftluent
,..cilmL ,..ci!mL Concentration
IE-16 9E-14 9.88E-01
IE-16 3E-14 3.04E-01
IE-16 9E-13 l.l?E-02
2E-15 6E-13 1.33E+00
Page 3 of 22
EI\ERGY .. , ,., . Htlel1, 1fT 177-472-1711 • Bllllnp, 1fT •t-735-4419 • Cuper, W'f 811-235-1511
Gilleltl. WY a.lll-7175 • Rapid City, SO 111-172-1225 • Celleae Station, TX 811-tiD-2211
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/11/13
Collection Date: 09/30/13
DateReceived: 10/07/13
Matrix: Filter
Project: 3rd Quarter Air 2013
LabiD: C13100250-001
Client Sample 10: BHV-1
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL-Quality control limit.
Result Units
0.179 mglfilter
121 pCii Filter
1090 pCiiFilter
18 pCiiFilter
5.9 pCi/Filter
14.4 pCiiFilter
1.3 pCiiFilter
0.2 pCiiFilter
12 pCiiFilter
3.9 pCi/Filter
2.4 pCiiFilter
MDC -Minimum detectable concentration
Qualifiers
MCLI
RL QCL Method Analysis Date I By
0.0003 SW6020 10130113 04:17 I cp
0.2 SW6020 10130113 04:17 I cp
E909.0 11106113 12:38 I eli-cs
E909.0 11106113 12:38 I eli-cs
E909.0 11106113 12:38 I eli-cs
E903.0 10122/13 21 :12 I lmc
E903.0 10122113 21 :12 I imc
E903.0 1 0122113 21 :12 I lmc
E908.0 10129113 09:04 I dmf
E908.0 1 0129113 09:04 I dmf
E908.0 10129113 09:04 I dmf
MCL -Maximum contaminant level.
ND-Not detected at the reporting limit.
Page 4 of 22
EN:RGY
I I ! !1 •
Ill*'•· liT 177-472-0711 • Blllinp, liT IGIJ.. 7Ji-4411 • Casper, WY 181·235-0515
Gillette, W'f 111-111·7175 • Rapid City, SD 11 ... 72·1225 • Colleie Station, TX 181·1111-2211
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: November 11,2013
PROJECT: 3rd Quarter Air 2013
SAMPLEID: BHV-2
Quarter/Date Sampled Concentration
Air Volume Radio nuclide 11CilmL
1 c 1304021 o-oo2 natu 3.38E-16
IFin;t Quarter 2013 2l'Th 3.94E-17
Air Volume in mLs 226Ra 8.32E-17
1.36E+ll 210Pb i.42E-14
Quarter/Date Sampled Concentration
Air Volume Radionuclide J1CilmL
Cl3070231-002 ""u 4.06E-16
I SecorHJ Quarter 20 13 2>0Th 4.89E-17
Air Volume in mLs 226Ra 8.06E-17
1.38E+ll 210Pb 4.93E-15
Quarter/Date Sampled Concentration
Air Volume Radio nuclide J1CilmL
C13!00250-002 natu 1.76E-16
Third Quarter 2013 23'Th 2.52E-l7
Air Volume in mLs 226Ra 6.13E-17
1.37E+11 210Pb 4.90E-15
+LLD's are from Reg. Guide 4.14
Counting
Precision
J1CilmL
N/A
IE-17
9E-18
2E-16
Counting
Precision
J1CilmL
N/A
IE-17
7E-18
IE-16
Counting
Precision
J1CilmL
N/A
lE-17
8E-18
!E-16
*Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDCJ1CilmL
N/A
9E-18
4E-18
SE-17
MDCJiCilmL
N/A
6E-18
3E-18
6E-17
MDC J1CilmL
N/A
9E-18
2E-18
4E-17
L.L.D.+ Effluent Cone.* %Effluent
J1CilmL J1CilmL Concentration
iE-16 9E-14 3.75E-OI
1E-l6 3E-14 1.31E-OI
IE-16 9E-13 9.25E-03
2E-15 6E-13 2.37E+00
L.L.D.+ Effluent Cone.* %Effluent
J1CilmL 11CilmL Concentration
IE-16 9E-14 4.51E-Ol
IE-16 3E-14 l.63E-OI
lE-16 9E-13 8.95E-03
2E-l5 6E-13 8.21E-OI
L.L.D! Effluent Cone.* %Effluent
J1CilmL 11CilmL Concentration
IE-16 9E-14 1.96E-OI
lE-16 3E-14 8.40E-02
IE-16 9E-13 6.81E-03
2E-15 6E-13 8.17E-Ol
Page 5 of 22
EI\ERGY
• • ' lit
Helell1, fliT 177-472-8711 • BillinJS, fliT 8GI· 135-4481 • Casper, WY 811-235-1515
Gillette, WV 111-111-7171 • Rapid City, SD 118-172·1225 • CGIIeae Station, 1X 811-1111-2211
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11 /11 /13
Collection Date: 09/30/13
DateReceived: 10/07/13
Matrix: Filter
Project:
labiD:
3rd Quarter Air 2013
c 131 00250-002
Client Sample ID: BHV-2
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL -Quality control limit.
Result Units
0.0355 mglfilter
24.0 pCiiFilter
670 pCiiFilter
14 pCiiFilter
5.9 pCi/Filter
8.4 pCi/Filter
1.1 pCi/Filter
0.2 pCiiFilter
3.4 pCiiFilter
1.5 pCi/Filter
1.2 pCi/Filter
MDC -Minimum detectable concentration
MCLI
Qualifiers RL QCL Method Analysis Date I By
0.0003 SW6020 1 0130113 04:29 I cp
0.2 SW6020 10130113 04:29 I cp
E909.0 11106113 13:48 1 eli-cs
E909.0 11106113 13:48 1 eli-cs
E909.0 11106113 13:48 I eli-cs
E903.0 10122113 21 :1211mc
E903.0 10122113 21 :1211mc
E903.0 10122/13 21 :1211mc
E908.0 10129113 09:041 dmf
E908.0 10129113 09:04 I dmt
E908.0 1 0129/13 09:04 I dmt
MCL-Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 6 of22
Er\ERGY
,. jO. •
llllena, MTI77-472-0711 • Billlnp, MT IOD-735-4411 • Casper, W'f 181-235-1515
Gillette, W'f 111-111·7171 • Rapid City, SD 188-172·1221 • Collese Station, TX 881-8BD·2211
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: November 11,2013
PROJECT: 3rd Quarter Air 2013
I
SAMPLE ID: BHV-4
Quarter/Date Sampled Concentration
Air Volume Radionuclide 11CilmL
c 1304021 0-003 natu 3.04E-15
I F'irsl Quarter 2013 230Th 4.99E-16
Air Volume in mLs 226Ra 2.79E-16
1.35E+ll 210Ph 2.13E-14
Quarter/Date Sampled Concentration Radionuclide Air Volume J1CilmL
C13070231-003 natu 2.50E-15
I second Quarter 2013 "!ll~l'h 3.62E-16
Air Volume in rnl..<; 226Ra 2.40E-16
1.37E+ll 210Pb 4.93E-15
Quarter/Date Sampled Concentration Radionuclide Air Volume 11CilmL
c 131 00250-003 ""U 2.98E-15
Third Quarter 2013 23~h 4.49E-16
Air Volume in mLs il6Ra 1.54E-16
1.35E+ll 210Pb 7.49E-15
+LLD's are from Reg. Guide 4.14
Counting
Precision
11CilmL
N/A
9E-17
2E-17
2E-16
Counting
Precision
11CilmL
N/A
5E-17
IE-17
IE-16
Counting
Precision
J1CilmL
N/A
8E-17
IE-17
IE-16
*Effluent Concentration from the NEW I 0 CFR Part 20 -Appendix B -Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radiurn-226
Day for Lead-210
MDC J1CilmL
N/A
2E-17
4E-18
5E-17
MDC 11CilmL
N/A
lE-17
3E-18
6E-17
MDC J1CilmL
N/A
2E-17
2E-18
4E-17
L.L.D.+ Effluent Cone.* %Effluent
11CilmL 11CilmL Concentration
IE-16 9E-14 3.38E+00
IE-16 3E-14 1.66E+00
IE-16 9E-13 3.10E-02
2E-15 6E-13 3.54E+00
L.L.D.+ Effluent Cone.* %Effluent
11CilmL 11CilmL Concentration
1E-16 9E-14 2.78E+00
IE-16 3E-14 1.21E+00
IE-16 9E-13 2.67E-02
2E-15 6E-13 8.22E-01
L.L.D.• Effluent Cone.* %Effluent
1JCilmL J1CilmL Concentration
1E-16 9E-14 3.31E+00
IE-16 3E-14 1.50E+00
1E-16 9E-13 1.71E-02
2E-15 6E-13 1.25E+00
Page 7 of22
EN:RGY
' .. · '
Helena, lilT 877--472-0711 • Billinp, MT BGI·Jal-4481 • Casper, WY 888-235-8511
Gilllth, W'r 118-118·7111 • Rapid City, SD 888-172·1221 • Collqe Station, IX 888-610·2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11 /11/13
Collection Date: 09/30/13
Date Received: 10/07/13
Matrix: Filter
Project: 3rd Quarter Air 2013
Lab 10: C13100250-003
Client Sample 10: BHV-4
Analyses
TRACE METALS
Uranium
Uranium, Activity
RAOIONUCLIDES
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL-Quality control limit.
Result Units
0.593 mgllilter
401 pCiiFilter
1010 pCi/Filter
17 pCiiFilter
5.8 pCi!Filter
20.8 pCiiFilter
1.6 pCiiFilter
0.2 pCiiFilter
61 pCiiFilter
11 pCi!Filter
2.5 pCiiFilter
MDC -Minimum detectable concentration
Qualifiers
MCLI
RL QCL Method Analysis Date I By
0.0003 SW6020 10130113 04:331 cp
0.2 SW6020 1 0130113 04:33 I cp
E909.0 11106113 14:57 I eli-cs
E909.0 11106113 14:57 I eli-cs
E909.0 11106113 14:57 I eli-cs
E903.0 10122113 21 :12 llmc
E903.0 10122/13 21:12 I lmc
E903.0 10122113 21 :1211mc
E908.0 10129113 09:04 I dmt
E908.0 1 0129113 09:04 I dml
E908.0 10129113 09:041 dmf
MCL -Maximum contaminant level.
NO-Not detected at the reporting limit.
Page 8 of 22
Helena, MT 177-472-0711 • Billln11, MT 100· 715-4411 • Casper, WY 181-235-0515
Gillette, W'f 118·811· 7171 • Rapid City, SD 118·872·1225 • Collqe Station, TX 181·180·2211
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: November 11,2013
PROJECT: 3rd Quarter Air 2013 • SAMPLE ID: BHV-5
Quarter/Date Sampled Concentration
Air Volume Radionuclide !JCi/mL
:c 13040210-004 nalu 6.66E-15
r:as~ Quarter 2013 23oTh 1.48E-15
Air Volume in mLs 226Ra 1.12E-15
1.35E+ll 210Pb 1.80E-14
Quarter/Date Sampled Concentration
Air Volume Radionuclide !JCilmL
C13070231-004 natu 7.35E-15
Second Quarter 2013 23~h 1.72E-15
Air Volume in mLs 226Ra 2.02E-15
1.37E+ 11 210Pb 6.67E-15
Quarter/Date Sampled Concentration
Air Volume Radionuclide !JCi/mL
C13100250-004 ""U 2.78E-15
Thirtl Quarter 2013 1JU.I11 6.92E-16
Air Volume in rnl..'i 4'6Ra 3.29E-16
1.35E+ll 210Pb 6.62E-15
+LLD's are from Reg. Guide 4.14
Counting
Precision
I!CilmL
NIA
3E-16
3E-17
2E-16
Counting
Precision
!JCi/mL
N/A
2E-16
4E-17
lE-16
Counting
Precision
!JCi/mL
NIA
SE-17
2E-17
IE-16
*Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDC!JCi/mL
N/A
4E-17
4E-18
SE-17
MDC!JCilmL
N/A
2E-l7
3E-18
6E-l7
MDC!JCilmL
N/A
3E-18
2E-18
4E-17
L.L.D.+ Effluent Cone.* %Effluent
!JCi/mL !JCI/mL Concentration
IE-16 9E-14 7.40E+00
IE-16 3E-14 4.95E+00
IE-16 9E-13 1.24E-OI
2E-15 6E-13 3.00E+00
L.L.D.+ Effluent Cone.* % Eftluent
11CilmL !JCi/mL Concentration
IE-16 9E-14 8.16E+00
tE-16 3E-14 5.74E+00
1E-16 9E-13 2.25E-01
2E-15 6E-13 l.IIE+OO
L.L.D.+ Effluent Cone.* %Effluent
!JCi/mL !JCilmL Concentration
IE-16 9E-14 3.09E+00
1E-16 3E-14 2.31E+00
IE-16 9E-13 3.65E-02
2E-15 6E-13 J.IOE+OO
Page 9 of 22
EN:RGY
•-•, • I I I
Helena, MT 177-472-0711 • Bllllnp, MT BGI-731-4411 • Cuper, WY 811-235-1515
Gillelte, WY 116-118-7175 • Rapid Cltr, SD 116-172-1225 • Colleee Station, 1X 118-IID-2211
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/11/13
Collection Date: 09/30/13
DateReceived: 10/07/13
Matrix: Filter
Project: 3rd Quarter Air 2013
Lab ID: c 131 00250-004
Client Sample ID: BHV-5
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL · Quality control limit.
Result Units
0.554 mg/lilter
375 pCi!Filter
893 pCii Filter
16 pCiiFilter
5.8 pCii Filter
44.3 pCi!Filter
2.4 pCii Filter
0.2 pCiiFilter
93 pCi!Filter
7.2 pCii Filter
0.43 pCii Filter
MDC -Minimum detectable concentration
Qualifiers
MCL!
RL QCL Method Analysis Date I By
0.0003 SW6020 1 0130113 04:54 I cp
0.2 SW6020 10/30113 04:54 I cp
E909.0 11106113 16:06 1 eli-cs
E909.0 11106113 16:061 eli-cs
E909.0 11106113 16:06 1 eli-cs
E903.0 10122113 21:12 11mc
E903.0 10122113 21 :12 11mc
E903.0 10122/13 21 :12 llmc
E908.0 1 0129113 16:43 I dmf
E908.0 10129113 16:43 I dmf
E908.0 10129113 16:43 I dmf
MCL-Maximum contaminant level.
ND-Not detected at the reporting limit.
Page 10 of 22
EN:RGY Helena, MT 877-472-11711 • Bllllnga, MT 800-735-4411 • C11per, WY 188·235·8115
Gillette, WY 111·811·7171 • Rapid City, SO 818-172·1225 • College Station, TX 181-1811-2211
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: November 11, 2013
PROJECT: 3rd Quarter Air 2013
SAMPLEID: BHV-6
Quarter/Date Sampled Concentration
Air Volume Radionuclide 11CilmL
C13040210-005 nalu 4.52E-15
First Quarter 2013 23oTh 7.93E-16
Air Volume in mL~ 226Ra 4.91E-16
1.35E+11 2IOPb l.?OE-14
Quarter/Date Sampled Concentration
Air Volume Radionuclide J1CilmL
C13070231-005 nalu 5.91E-15
Second Quarter 20 13 ~"rh 6.74E-l6
Air Volume in mL~ nnRn 7.85E-16
1.37E+11 2JOPb 5.18E-15
Quarter/Date Sampled Concentration Radionuclide Air Volume 11CilmL
ICJ3!00250-005 nalu 2.68E-15
'Thi1'd Quarter 2013 2JoTh 3.97E-16
Air Volume in ntl.s W1Ra 1.04E-16
1.35E+ll 210Pb 6.13E-15
+LLD's are from Reg. Guide 4.14
Counting
Precision
J1CilmL
N/A
2E-16
2E-17
2E-16
Counting
Precision
J1CilmL
N/A
9E-17
2E-17
1E-16
Counting
Precision
J1CilmL
N/A
IE-16
1E-17
1E-16
*Effluent Concentration from the NEW I 0 CFR Part 20 -Appendix B -Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDCJ1CilmL
N/A
4E-17
4E-18
6E-17
MDC J1CilmL
N/A
2E-17
3E-18
6E-17
MDC1JCilmL
N/A
4E-17
2E-18
4E-17
L.L.D.+ Effluent Cone.* %Effluent
11CilmL 11CilmL Concentration
IE-16 9E-14 5.02E+00
1E-16 3E-14 2.64E+00
JE-16 9E-13 5.46E-02
2E-15 6E-13 2.83E+00
L.L.D.+ Effluent Cone.* %Effluent
11CilmL 11CilmL Concentration
1E-16 9E-l4 6.57E+00
lE-16 3E-14 2.25E+00
IE-16 9E-13 8.73E-02
2E-15 6E-13 8.64E-Ol
L.L.D.+ Effluent Cone.* %Effluent
11CilmL J1CilmL Concentration
IE-16 9E-14 2.97E+00
IE-16 3E-14 1.32E+00
1E-16 9E-13 1.16E-02
2E-15 6E-13 1.02E+00
Page 11 of 22
Helena, MT 877-4 72-0711 • Bllllnp, MT 881· 131-4481 • Caspar, WY 818-235-1515
Glllt!U, WY 118-188·7171 • Rapid City, SD 188-172·1225 • Collqe Station, IX 811-110.2211
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/11 /13
Collection Date: 09/30/13
DateReceived: 10/07/13
Matrix: Filter
Project: 3rd Quarter Air 2013
Lab ID: C131 00250-005
Client Sample ID: BHV-6
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 210 precision(±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL-Quality control limit.
Result Units
0.532 mglfilter
360 pCiiFilter
824 pCiiFilter
16 pCi/Filter
5.8 pCiiFilter
14.0 pCiiFilter
1.3 pCiiFilter
0.2 pCi/Filter
53 pCiiFilter
13 pCiiFilter
5.8 pCi/Filter
MDC -Minimum detectable concentration
Qualifiers
MCLI
RL QCL Method Analysis Date I By
0.0003 SW6020 10130113 05:03 1 cp
0.2 SW6020 10130/13 05:03 / cp
E909.0 11106113 17:16 1 eli-cs
E909.0 11106113 17:16 I eli-cs
E909.0 11106113 17:16 I eli-cs
E903.0 1 0/22113 21 :1211mc
E903.0 10122113 21 :12 11mc
E903.0 10122/13 21 :12 11mc
E908.0 10129/13 09:041 dmf
E908.0 10129113 09:041 dmf
E908.0 10129113 09:04/ dmf
MCL -Maximum contaminant level.
ND-Not detected at the reporting limit.
Page 12 of 22
Er\ERGY ... ~ . ·. .
Helene, liT 877-472·0711 • Bllllnes, liT 8110·71D-4411 • Casper, WY 181-%35-0515
Gillette, WY 811·818·7178 • Rapid City, SO 811·172·1225 • CoiJeee Station, TX 181-111-2211
illGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: November 11, 2013
PROJECT: 3rd Quarter Air 2013
SAMPLE ID: Blank
Quarter/Date Sampled Concentration Radionuclide Air Volume J.lCi/mL
c 13040210-006 nalu 9.60E-18
FIN~1 Quarter 2013 l..>aTh 3.27E-18
Air Volume in mU; 22-6Rn 3.89E-18
1.36E+I1 210Pb -4.09E-J7
Counting
Precision
J.1CilmL
N/A
3E-18
3E-18
3E-17
Note: This ~11mple uses 136100 0,00 0 L of air volume for comp11rison JHII'poses.
Quarter/Date Sampled Concentration Counting
Air Volume Radionuclide J.lCi/mL Precision
J.1CilmL
IC13070231-006 ~·u 7.23E-18 N/A
Second Quarter 20 13 2JoTh 7.06E-18 2E-18
Air Volume in mLs 226Ra 4.52E-18 2E-18
1.36E+11 210Pb -7.38E-18 4E-17
Note: This sample. uses 136,000,()00 L of air volume for comJlnrls(ln purposes.
Quarter/Date Sampled Concentration Counting
Radionuclide Precision Air Volume 1JCilmL 1JCilmL
IC13100250-006 natu 9.41E-18 N/A
Third Quarter 2013 2JoTh 5.84E-18 SE-18
Air Volume in mLs 226Ra 3.64E-18 2E-18
1.36E+ll 210Pb 1.34E-18 3E-17
Note: Th1s sample uses 136,000,000 L of mr volume for companson purposes.
+LLD's are from Reg. Guide 4.14
*Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day forLead-210
MDC J.1CilmL
N/A
6E-18
4E-18
SE-17
MDC J.1CilmL
NIA
2E-18
3E-18
6E-17
MDCJ.1CilmL
NIA
7E-18
2E-18
4E-17
L.L.D.+ Effluent Cone.* %Effluent
J.lCi/mL J.lCi/mL Concentration
1E-16 9E-14 1.07E-02
lE-16 3E-14 1.09E-02
lE-16 9E-l3 4.32E-04
2E-15 6E-l3 -6.82E-03
L.L.D.+ Effluent Cone.* %Effluent
jJCilmL 1JCi/mL Concentration
1E-16 9E-14 8.03E-03
IE-16 3E-14 2.3SE-02
IE-16 9E-13 S.02E-04
2E-1S 6E-l3 -1.23E-03
L.L.D! Effluent Cone.* %Effluent
jJCi/mL J.1CilmL Concentration
IE-16 9E-14 I.OSE-02
IE-16 3E-14 1.95E-02
lE-16 9E-13 4.05E-04
2E-15 6E-13 2.23E-04
Page 13 of 22
EI\ERGY
I"" "\ I • ' ~ ! •
Helene, MT 877 .. n2-G711 • Blllln&~, MT 8GI·73S-4481 • Casper, WY 81J.235-151S
Gillette, WY 811-118·7171 • Rapid City, SD 811-172·1225 • Colleae Station, 1X 811-&10-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 11/11/13
Collection Date: 09/30/13
Date Received: 1 0/07/13
Matrix: Filter
Project: 3rd Quarter Air 2013
Lab ID: c 131 00250-006
Client Sample ID: Blank
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 210 precision(±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL-Quality control limit.
Result Units
0.0019 mglfilter
1.3 pCiiFilter
0.18 pCiiFilter
3.4 pCiiFilter
5.8 pCiiFilter
0.5 pCiiFilter
0.3 pCiiFilter
0.2 pCiiFilter
0.79 pCiiFilter
0.65 pCi/Filter
1.0 pCiiFilter
MDC -Minimum detectable concentration
Qualifiers
u
u
MCLI
RL QCL Method
0.0003 SW6020
0.2 SW6020
E909.0
E909.0
E909.0
E903.0
E903.0
E903.0
E908.0
E908.0
E908.0
Analysis Date I By
10130113 05:07 I cp
10130113 05:07 I cp
11106113 18:25 I eli-cs
1110611318:251eli-cs
11106113 18:25 I eli-cs
10122113 21 :12 I lmc
1 0122113 21 :12 I lmc
10122113 21 :12 I lmc
1 0129113 09:04 I dmf
1 0129113 09:04 I dmf
1 0129113 09:04 I dmf
MCL -Maximum contaminant level.
NO-Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Page 14 of 22
Helena, MT 177-472..CJ711 • Blllinp, MT IGI· 731-44H • Casper, WY 811-235-1115
Glllltta, WY 118-188· 7171 • Rapid City, SD 111-172·1225 • Coll&ge Station, TX 811-8111-2211
QAJQC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 3rd Quarter Air 2013
Analyte Count Result Units
Method: E903.0
Sample ID: C13100312-001HMS
Radium 226
Sample ID: C13100312·001HMSD
Radium 226
Sample ID: LCS-39399
Radium 226
Sample ID: MB-39399
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Qualifiers:
RL-Analyte reporting limit.
3
MDC -Minimum detectable concentration
Sample Matrix Spike
18 pCi/L
Sample Matrix Spike Duplicate
18 pCi/L
Laboratory Control Sample
23.3 pCi/Filter
Method Blank
0.4 pCi/Filter
0.2 pCi/Filter
0.1 pCi/Filter
Report Date: 11/11/13
Work Order: C131 00250
RL %REC Low Limit High Limit RPD RPDLimit Qual
Run: BERTHOLD 770-2_131016A
95 70 130
Run: BERTHOLD 770-2_131 016A
97 70 130 1.8
Run: BERTHOLD 770-2_131 016A
107 80 120
Run: BERTHOLD 770-2_131016A
NO -Not detected at the reporting limit.
Batch: 39399
10/22/13 22:57
10/22/13 22:57
22.4
10/22/13 22:57
10/22/13 22:57
Page 15 of 22
EN:RGY
· ,....• j,.-.,, II' ,
Helm, MT 877-472-8711 • Bllll•p, MT IGI-731-4481 • Casper, WY 888-235-1511
Gillette, WY 818-188-7115 • Rapid City, SD 118-172-1225 • Colleie Station, TX 811-tll-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 3rd Quarter Air 2013
Analyte Count Result Units
Method: E908.0
Sample ID: C131 00250-001 ADUP 3 Sample Duplicate
Thorium 230 16.2 pCi/Filter
Thorium 230 precision (±} 4.42 pCi/Filter
Thorium 230 MDC 2.48 pCi/Filter
Sample ID: C13100250·006AMS Sample Matrix Spike
Thorium 230 77.6 pCi/Filter
Sample ID: MB-39399 3 Method Blank
Thorium 230 0.10 pCi/Filter
Thorium 230 precision (±) 0.2 pCi/Filter
Thorium 230 MDC 0.5 pCi/Filter
Sample ID: LCS-39399 Laboratory Control Sample
Thorium 230 19.1 pCi/Filter
Method: E908.0
Sample ID: C131 00250·004AM S Sample Matrix Spike
Thorium 230 2.09E-06 pCi/Filter
Sample ID: C13100250·004AMSD Sample Matrix Spike Duplicate
Thorium 230 2.19E-06 pCi/Filter
Sample ID: MB-39399 3 Method Blank
Thorium 230 0.2 pCi/Filter
Thorium 230 precision (±} 0.09 pCi/Filter
Thorium 230 MDC 0.1 pCi/Filter
Sample ID: LCS-39399 Laboratory Control Sample
Thorium 230 19.6 pCi/Filter
Qualifiers:
RL-Analyte reporting limit.
MDC -Minimum detectable concentration
Report Date: 11/11/13
Work Order: C13100250
RL %REC Low Limit High Limit RPD RPDLimlt Qual
Run : ALPHANALYST_131021A
26
Run: ALPHANALYST_131021A
100 70 130
Run: ALPHANALYST_131021A
Run: ALPHANAL YST_131021A
105 80 120
Run: ALPHANALYST_131028A
96 70 130
Run: ALPHANAL YST _131 028A
105 70 130 4.3
Run: ALPHANAL YST_131028A
Run: ALPHANALYST_131028A
107 80 120
NO-Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Batch: 39399
1 0/29/13 09:04
67.3
10/29/13 09:04
10/29/13 09:04
u
1 0/29/13 09:04
Batch: 39399
10/29/1316:43
1 0/29/13 16 :43
25.4
10/29/13 16:43
1 0/29/13 16 :43
Page 16 of 22
Helen•, MT 877-472-1711 • Bllllnp, MT 101·731-4488 • Casper, WY 811-235-1111
Gillette, WY 111-188·7171 • Rapid City, SD 111-172·1225 • CollegeStltlon, 1X 111-118-2211
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 3rd Quarter Air 2013
Analyte
Method: E909.0
Sample ID: LCS-19796
Lead 210
Sample ID: MB-19796
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Sample ID: T13100052-001HMS
Lead 210
Sample ID: T13100052-001HMSD
Lead 210
Qualifiers:
RL-Analyte reporting limit.
Count Result Units
Laboratory Control Sample
120 pCi/L
3 Method Blank
-2
3
6
pCi/L
pCI/L
pCI/L
Sample Matrix Spike
66 pCi/L
Sample Matrix Spike Duplicate
80 pCi/L
MDC-Minimum detectable concentration
Report Date: 11/11/13
Work Order: C13100250
RL %REC Low Limit High Limit
Run: SUB-T53838
93 80 120
Run: SUB-T53838
Run: SUB-T53838
84 70 130
Run: SUB-T53838
101 70 130
NO-Not detected at the reporting limit.
RPD RPDLimit Qual
18
Batch: T _19796
11/06/13 06:51
11/06/13 08:01
u
11/06/1310:19
11/06/13 11:29
21.1
U -Not detected at minimum detectable concentration
Page 17 of22
Heltu, MT871-472-G111 • Blllinp, MT 801·731-4481 • Catp81', WY 811-235-1511
GIIIJtta, WY 118-188·7175 • Rapid City, SD 118-172-1225 • Colleae Stltlon, TXIII-811-2211
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 3rd Quarter Air 2013
Report Date: 11/11/13
Work Order: C13100250
Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual
Method: SW6020 Analytical Run: ICPMS4-C_131029A
Sample 10: ICV Initial Calibration Verification Standard 10/29/13 16:44
Uranium 0.0511 mg/L 0.00030 102 90 110
Sample 10: ICSA Interference Check Sample A 10/29/1316:48
Uranium 4.73E-05 mg/L 0.00030
Sample 10: ICSAB Interference Check Sample AB 10/29/13 16:52
Uranium 1.23E-05 mg/L 0.00030
Method: SW6020 Batch: 39399
Sample 10: MB-39399 Method Blank Run: ICPMS4-C_131029A 10/30/13 04:04
Uranium NO mg/filter 0.0004
SampleiO: LCS2-39399 Laboratory Control Sample Run: ICPMS4-C_131029A 10/30/13 04:08
Uranium 0.0454 mg/filter 0.00030 45 85 115 s
-Response is below standard QA limit. This could indicate a low bias for the sample results. The sample results were confirmed by re-analysis of the sample, and
remaining batch QC recovery was acceptable. This batch is approved.
Sample 10: C13100250-001AMS Sample Matrix Spike Run: ICPMS4-C_131029A 10/30/13 04:21
Uranium 0.692 mg/filter 0.00030 108 75 125
Sample 10: C13100250-001AMSO
Uranium
Sample 10: C13100250-004AOIL
Uranium
Qualifiers:
RL-Analyte reporting limit.
MDC-Minimum detectable concentration
Sample Matrix Spike Duplicate
0.705 mg/filter
Serial Dilution
0.550 mg/filter
Run: ICPMS4-C_131029A
0.00030 111 75 125
Run: ICPMS4-C_131029A
0.00043
NO -Not detected at the reporting limit.
S -Spike recovery outside of advisory limits.
1.8
0,8
10/30/13 04:25
20
10/30/13 04:59
20
Page 18 of22
EN:RGY Helena, MT877-472-CI711 • Bllllnp, MTICII·131"'"H • Cuper, WY 811-235-1111
Gllltttl, WY 111-118· 7171 • Rapid City, SD 111-172·1221 • CGiteaa Station, IX IIJ.IID-2211
Workorder Receipt Checklist
Energy Fuels Resources (USA) Inc
Login completed by: Corinne Wagner
Reviewed by: BL2000\khelm
Reviewed Date: 10/8/2013
Shipping container/cooler in good condition?
Custody seals intact on all shipping container(s)/cooler(s)?
Custody seals intact on all sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
(Exclude analyses that are considered field parameters
such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.)
Temp Blank received in all shipping container(s)/cooler(s)?
Container/Temp Blank temperature:
Water-VOA vials have zero headspace?
Water-pH acceptable upon receipt?
Yes 0
Yes D
Yes D
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes D
N/A'C
Yes D
Yes D
C13100250
Date Received: 10/7/2013
Received by: cav
NoD
NoD
NoD
No 0
No 0
No 0
No 0
NoD
NoD
NoD
NoD
NoD
NoD
Carrier Next Day Air
name:
Not Present D
Not Present 0
Not Present 0
Not Applicable 0
NoVOA vials submitted 0
Not Applicable 0
______ ,.. ______ ,. __________________ ---------------------------~---------------------
------·----------------·--~--------------------.. ---------------------------------
Standard Reporting Procedures:
Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as
pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time.
Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected,
data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried
and ground prior to sample analysis.
Contact and Corrective Action Comments:
None
Page 19 of 22
Sheet 1 of 1
CHAIN OF CUSTODY
Samples Shipped to: Energy Laboratories Contact: Garrin Palmer -=2'='as~a="'s~a~lt~c='r;.;..e"'-:ek~H;;.,;;wy ___ ........____ Ph: 435 678 2108
Casper WY, 82601 [e-mail]
Chain of Custody/Sampling Analysis Request
Project
3rd Quarter Air
SampleiD Date Collected
BHV-1 7/2/13-10/1/13
BHV-2 7/2113-10/1/13
BHV-4 7/2113-10/1/13
BHV-5 7/2/13-10/1/13
BHV-6 7/2/13-1011/13
Blank 7/2/13-10/1/13
Comments:
Relinq~ished By:(~a~re)
c;~~~-
Relinquished By:(Signature)
Samplers Name Samplers Signature
Garrin Palmer
Time
Collected Laboratory Analysis Requested
NA U-NAT, Th-230, Aa-226, Pb-210
NA U-NAT, Th-230, Ra-226, Pb-210
NA U-NAT, Th-2.30, Ra-226, Pb-210
NA U-NAT, Th-230, Ra-226, Pb-210
NA U-NAT, Th-230, Ra-226. Pb-210
NA U-NAT, Th-230, Ra-226, Pb-210
Datemme Received By:(Signature)
10/4/2013
1100
Date/Time
Date/Time
Page 20 of22
EJ\ERGY
.... j 1"1 •
www.energylab.com
AltllfiJal E.lallla ar:. rm
Helen1, MT 871_.12..0711 • Billinp, MT 801-131-4411 • Caspar, WY 811-235-1111
Gillette, WV 111-&86· 7175 • Rapid City, SD 111-172· 1225 • Collate Station, TX 118-&10-2211
February 06, 2014
Energy Fuels Resources (USA) Inc
225 Union Blvd Ste 600
Lakewood, CO 80228-1826
Workorder No.: C14010034
Project Name: 4th Quarter Air 2013
ANALYTICAL SUMMARY REPORT
Energy Laboratories, Inc. Casper WY received the following 6 samples for Energy Fuels Resources (USA) Inc on 1/3/2014 for
analysis.
Sample ID Client Sample ID Collect Date Receive Date Matrix Test
C1401 0034-001 BHV-1 12/30/13 00 :00 01 /03/14 Filter Composite of two or more samples
Metals, Total
Digestion, Total Metals
RAD Alternate Unit Reporting Air
Filters
C1401 0034-002 BHV-2
C14010034-003 BHV-4
C1401 0034-004 BHV-5
C1401 0034-005 BHV-6
C 1401 0034-006 Blank
12/30/13 00 :00 01 /03/14
12/30/13 00:00 01 /03/14
12/30/13 00:00 01 /03/14
12/30/13 00:00 01 /03/14
12/30/13 00:00 01/03/14
Filter
Filter
Filter
Filter
Filter
Lead 210
Radium 226
Thorium, Isotopic
Same As Above
Same As Above
Same As Above
Same As Above
Same As Above
The results as reported relate only to \he ltem(s) submitted for testing. The analyses presented In this report Were
performed at Energy Laboratories, Inc., 2393 Salt .Creek Hwy., Casper, WY 82601, unless otherwise noted.
8adlochemistry analyses were p'ertormed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601,
unless otherwise noted. Any exceptions or problems with the analyses are noted In thE! Laboratory Analytical
Repcrt, the QAIQC Summary.Heport, or the Case Narrative.
If you have any questions regarding these test results, please call.
Digitally signed by
Steve Carlston Report Appcoved By: ~ ~ ~
/ Interim Branch Manager
Date: 2014.02.06 17:25:13 -07:00
Page 1 of 22
EI\ERGY
' .
Helena, MT 877-472-0711 • Bllllnp, MT 801-735-4481 • Cuper, WY 811-235-0515
Gillette, WY IIB-111-7175 • Rapid Ctty, SD 111-172-1225 • College Statton, TX 811-110·2211
CLIENT: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Air 2013
Sample Delivery Group: C14010034
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Report Date: 02/06/14
CASE NARRATIVE
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this
method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should
be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of
counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven
individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB
monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
e/1-b -Energy Labora~orles, Inc. • Billings, MT
·eti-g-Energy Laboratories, Inc.-Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
e.ll·r • Energy Laboratories, Inc. -Rapid City, SD
eli-cs -Energy Laboratories, Inc. • CoHege Stalion, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERCSY LABORATORIES~ INC.· CASPEB,WY certifies lhatcertaln method selections contained in this report meet
r~uirem.ents as set forth by the at>p~e accrediting authorities. Some results requested by the client may not be covered under
1hese oert!fi.Gatlons. All analysis data to be submitte(l for cegul~tory enforcement should be certified in the sample state of
origin. Please verily ELl's certification coverage-by visiting www.energylab.com
Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web
page www.energylab.com.
Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College
Station, TX, EPA Number TX01520.
Page 2 of22
www.anergyleb.com
AlllllfJrM ,..,_ Sillclll!fl
Helena, MT 177-472-0711 • Billings, MT 101-735-4411 • Casper, WY 888·235-8515
Gillette, WY 8&1·881-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 881·&90-2218
IDGH VOLUME AIR SAMPLING REPORT
•
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: February 6, 2014
PROJECT: 4th Quarter Air 2013
SAMPLE ID: BHV-1
Quarter/Date Sampled Concentration
Air Volume Radionuclide JJCilmL
Cl3040210-001 nalu 9.91E-16
First Quarter 20 13 230Th l.86E-16
Air Volume in mLs 226Ra 2.04E-16
l.36E+ll 210Pb 1.82E-14
Quarter/Date Sampled Concentration Radionuclide Air Volume J!CilmL
Cl3070231-001 ""U l.46E-15
Second Quarter 2013 23oTh 3.34E-16
Air Volume in mLs 226Ra 3.91E-16
1.34E+l1 210Pb 5.78E-15
Quarter/Date Sampled Concentration Radionuclide Air Volume JJCilmL
Cl3100250-001 ""U 8.89E-16
Third Qumter 20 13 230Th 9.13E-17
Air Volume in rnL~ 226Ra l.OSE-16
1.37E+ll 210Pb S.OOE-15
Quarter/Date Sampled Concentration Radionuclide Air Volume JJCilmL
Cl4010034-001 ""U 5.21E-16
Fourth Quarter 20 13 230Th 4.34E-17
Air Volume in mLs 226Ra 3.70E-17
l.35E+ll 210Pb 2.59E-14
+LLD's are from NRC Reg. Guide 4.14
Counting
Precision
J!CilmL
N/A
5E-l7
1E-l7
2E-16
Counting
Precision
JJCilmL
N/A
5E-17
2E-17
lE-16
Counting
Precision
JJCilmL
N/A
3E-17
IE-17
lE-16
Counting
Precision
JJCilmL
N/A
2E-17
8E-18
3E-16
*Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDC J!CilmL
N/A
2E-l7
4E-18
5E-17
MDCJJCilmL
N/A
2E-17
3E-18
6E-17
MDC J!CilmL
N/A
2E-17
2E-18
4E-17
MDCJJCilmL
N/A
3E-17
SE-18
6E-17
-...
L.L.D.+ Effluent Cone.* %Effluent
JJCilmL JJCilmL Concentration
1E-16 9E-14 l.IOE+OO
lE-16 3E-14 6.21E-01
IE-16 9E-13 2.27E-02
2E-15 6E-13 3.03E+00
L.L.D.+ Eftluent Cone.* %Effluent
J!CilmL JJCilmL Concentration
lE-16 9E-14 1.62E+00
IE-16 3E-14 l.llE+OO
lE-16 9E-13 4.35E-02
2E-15 6E-l3 9.64E-Ol
L.L.D.• Effluent Cone.* %Effluent
JJCilmL JJCilmL Concentration
lE-16 9E-14 9.88E-Ol
IE-16 3E-14 3.04E-01
lE-16 9E-13 l.l7E-02
2E-15 6E-13 l.33E+00
L.L.D.• Effluent Cone.* %Effluent
JJCilmL J!CilmL Concentration
lE-16 9E-14 5.78E-OI
lE-16 3E-14 1.45E-Ol
IE-16 9E-13 4.11E-03
2E-15 6E-l3 4.31E+00
Page 3 of 22
EN:RGY
• " I _ ,•1
www.energylab.com
,.,.. Eallll.w ... ,.
Helena, MT 817-472..0711 • Bllllnp, MT 801-735-4481 • Caspar, WY 811·23H515
Gilllltta, WY 111-111-7115 • Rapid City, SD 118-172-1225 • Collep Station, TX 811-&IG-2211
LABORATORY ANAL VTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Air 2013
Lab ID: c 1401 0034-001
Client Sample ID: BHV-1
Analyses
TRACE METALS ·IN AIR
Uranium
Uranium, Activity
RADIONUCLIDES • IN AIR
Lead 210
Lead 210 precision(±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
RADIONUCLIDES • IN AIR • PER FILTER
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Uranium, Activity
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
7.7E-10 mgiL
5.2E-16 uCilmL
2.6E-14 uCilmL
2.8E-16 uCilmL
6.1E-17 uCilmL
3.7E-17 uCi/mL
7.7E-18 uCilmL
5.3E-18 uCilmL
4.3E-17 uCilmL
2.4E-17 uCilmL
2.8E-17 uCilmL
3490 pCiiFilter
37.3 pCiiFilter
8.2 pCiiFilter
5.0 pCiiFilter
1.0 pCiiFilter
0.72 pCi/Filter
5.8 pCiiFilter
3.3 pCi/Filter
3.8 pCiiFilter
70.1 pCiiFilter
MDC -Minimum detectable concentration
Qualifiers
MCL/
Rl QCL
1.5E-10
1.0E-16
0.20
Report Date: 02/06/14
Collection Date: 12/30/13
DateReceived: 01/03/14
Matrix: Filter
Method Analysis Date I By
SW6020 01110114 00:451 elm
SW6020 01110114 00:451clm
E909.0 01122114 22:211 eli-cs
E909.0 01122114 22:21 I eli-cs
E909.0 01122114 22:211 eli-cs
E903.0 01120114 06:50 I lmc
E903.0 01120114 06:50 I lmc
E903.0 01120114 06:50 I lmc
E908.0 01114114 12:00 I dmf
E908.0 0111411412:00idmf
E908.0 01114114 12:00 I dmf
RADCALC 0210111413:021 sec
RADCALC 02101114 13:02 I sec
RADCALC 02101114 13:02 I sec
RADCALC 0210111413:021 sec
RADCALC 02101114 13:021 sec
RADCALC 02101114 13:02 I sec
RADCALC 02/0111413:021 sec
RADCALC 02101114 13:021 sec
RADCALC 02101114 13:02 I sec
RADCALC 02/01114 13:02 I sec
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 4 of22
EI\ERGY -::4 .. ,. ~-www.energyfab.com
~r......-.rw
Halene, MT 877-472-0711 • Billings, MT 800-735-4411 • Casper, WY 888-235-0515
Gllletta, W'f 88&-688-7175 • Rapid City, SD 888·172·1225 • Collage Station, lX 888-&90-2218
lllGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: February 6, 2014
PROJECT: 4th Quarter Air 2013 • SAMPLE ID: BHV -2
Quarter/Date Sampled Concentration
Air Volume Radionuclide f.ICilmL
c 13040210-002 ""U 3.38E-16
Fir 't Quarter 2 0 13 2JOTh 3.94E-17
Air Volume in mLs :ll~Ril 8.32E-17
1.36E+II 21UPb 1.42E-14
Quarter/Date Sampled Concentration
Air Volume Radionuclide f.ICilmL
'-' 3070231-002 ""U 4.06E-16
Sc~O!ld Quarter 2013 2J~h 4.89E-17
Air Volume in ru~~ 226Ra 8.06E-17
1.38E+11 210Pb 4.93E-15
Quarter/Date Sampled Concentration Radionuclide Air Volume 1JCilmL
Cl3100250-002 "''u 1.76E-16
Third Quarter 20 13 llrl>n1 2.52E-17
Air Volume in mLs 226Ra 6.13E-17
1.37E+ 11 2roPb 4.90E-15
Quarter/Date Sampled Concentration Radionuclide Air Volume f.ICilmL
c 14010034-002 nalu 6.20E-16
Fourt)l Quarter 2013 2JOTh 4.19E-17
Air Volume in mL~ 226Ra 3.72E-17
1.35E+ll 210Pb 2.50E-14
+ll.D's are from NRC Reg. Guide 4.14
Counting
Precision
f.ICilmL
N/A
lE-17
9E-18
2E-16
Counting
Precision
f.ICilmL
N/A
IE-17
7E-18
IE-16
Counting
Precision
f.ICilmL
N/A
lE-17
8E-18
IE-16
Counting
Precision
f.ICilmL
N/A
2E-17
8E-18
3E-16
*Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day forLead-210
MDCf.ICilmL
N/A
9E-18
4E-18
SE-17
MDCf.ICilmL
N/A
6E-18
3E-18
6E-l7
MDCf.ICilmL
N/A
9E-18
2E-18
4E-l7
MDCJJCilmL
N/A
2E-17
6E-18
6E-17
L.L.D.+ Effluent Cone.* %Effluent
f.ICilmL f.ICilmL Concentration
1E-16 9E-14 3.75E-01
lE-16 3E-14 1.3lE-01
lE-16 9E-13 9.25E-03
2E-15 6E-13 2.37E+00
L.L.D.+ Eftluent Cone.* %Effluent
,..cilmL 1JCilmL Concentration
IE-16 9E-14 4.5lE-Ol
lE-16 3E-14 1.63E-Ol
lE-16 9E-13 8.955-03
2E-15 6E-13 8.21E-OI
L.L.D.+ Effluent Cone.* %Effluent
f.ICi/mL f.ICilmL Concentration
lE-16 9E-14 1.96E-OI
1E-16 3E-14 8.40E-02
1E-16 9E-13 6.81E-03
2E-15 6E-l3 8.17E-OI
L.L.D,+ Effluent Cone.* %Effluent
f.ICilmL 1JCilmL Concentration
IE-16 9E-14 6.89E-OI
1E-16 3E-14 1.40E-Ol
lE-16 9E-13 4.13E-03
2E-15 6E-13 4.17E+00
Page 5 of 22
EI\ERGY
I \ II I , ,
www.energylab.com
bl/fiJG/ £lalla .. tift
Helene, MT 171-4U-G711 • Billinp, MT BGI-735-4419 • Casper, WY 811·235-1515
Gillette, WY 116-111-717! • Rapid City, SD 188-172-1225 • Collage Station, TX 888-&ID-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Air 2013
LabiD: c 1401 0034-002
Client Sample ID: BHV-2
Analyses
TRACE METALS -IN AIR
Uranium
Uranium, Activity
RADIONUCLIDES-IN AIR
Lead 210
Lead 210 precision(±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
RADIONUCLIDES -IN AIR -PER FILTER
Lead 210
Lead 210 precision(±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Uranium, Activity
Report
Definitions:
RL • Analyte reporting limit.
QCL-Quality control limit.
Result Units
9.2E-10 mgll
6.2E-16 uCilmL
2.5E-14 uCilmL
2.7E-16 uCilmL
6.1E-17 uCilmL
3.7E-17 uCilmL
8.0E-18 uCilmL
5.7E-18 uCilmL
4.2E-17 uCi/mL
1.7E-17 uCi/mL
1.5E·17 uCilmL
3370 pCiiFilter
36.8 pCiiFilter
8.2 pCiiFilter
5.0 pCiiFilter
1.1 pCiiFilter
0.77 pCiiFilter
5.6 pCiiFilter
2.3 pCiiFilter
2.1 pCiiFilter
83.5 pCiiFilter
MDC -Minimum detectable concentration
Qualifiers
MCL/
RL CCL
1.5E-10
1.0E-16
0,20
Report Date: 02/06/14
Collection Date: 12/30/13
DateReceived: 01/03/14
Matrix: Filter
Method Analysis Date I By
SW6020 01110114 00:481 elm
SW6020 01110114 00:48 I elm
E909.0 01122114 23:30 I eli-cs
E909.0 01122114 23:30 I eli-cs
E909.0 01122114 23:30 I eli-cs
E903.0 01120114 06:50 lime
E903.0 01120114 06:50 l ime
E903.0 01120114 06:50 lime
E908.0 0111411412:00 I dmf
E908.0 01114114 12:00 I dmf
E908.0 01114114 12:00 I dmf
RADCALC 0210111413:021 sec
RADCALC 02101114 13:02 I sec
RADCALC 02/01114 13:021 sec
RADCALC 02/0111413:021 sec
RADCALC 02101 11 4 13:02 I sec
RADCALC 02/01114 13:021 sec
RADCALC 02/0111413:021 sec
RADCALC 02101114 13:021 sec
RADCALC 02101114 13:021 sec
RADCALC 02101114 13:02 I sec
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 6 of22
EI\ERGY www.enefiYiab.com
~£iafllcl,-. IIJI
Helena, MT 817-472-0711 • Billings, MT BOD-735--«89 • Caspar, WY 888·235-0515
Glllatta, WY 86&-&8&-7115 • Rapid City, SO 8118·1112·1225 • Collage Station, lX 11811·&91-2218
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: February 6, 2014
PROJECT: 4th Quarter Air 2013
SAMPLE ID: BHV ·4
Quarter/Dale Sampled Concentration Radionuclide Air Volume 11CilmL
Cl3040210-003 nalu 3.04E-15
First Quarter 2 0 13 ~~.,) 4.99E-16
Air Volume in mLs .22b.Rn 2.79E-16
1.35E+ll 210Pb 2.13E-14
Quarter/Dale Sampled Concentration
Air Volume Radionuclide 11CilmL
IC1307023 J -003 natu 2.50E-15
Second Quarter 2013 23Drh 3.62E-16
Air Volume in mLs 226Ra 2.40E-16
1.37E+ll zwPb 4.93E-15
Quarter/Date Sampled Concentration Radionuclide Air Volume 11CilmL
iC13100250-003 nalu 2.98E-15
Third Quarter 20 13 23Drh 4.49E-16
Air Volume in mLs 226Ra 1.54E-16
1.35E+ll 210pb 7.49E-15
Quarter/Date Sampled Concentration Radio nuclide Air Volume 11CilmL
C14010034-003 ""U 3.88E-15
Fourth Quarter 2013 u 'Th 1.03E-16
Air Volume in mLs ~Ra 4.47E-17
1.34E+ll 2JOPb 2.93E-14
+LLD's are from NRC Reg. Guide 4.14
Counting
Precision
11CilmL
NIA
9E-17
2E-17
2E-16
Counting
Precision
11CilmL
NIA
SE-17
1E-J7
lE-16
Counting
Precision
11CilrnL
N/A
8E-17
1E-17
IE-16
Counting
Precision
11CilmL
N/A
4E-17
9E-18
3E-16
*Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
DayforLead-210
MDC 11CilrnL
N/A
2E-17
4E-18
SE-17
MDC 11CilrnL
N/A
1E-17
3E-18
6E-17
MDC11CilrnL
N/A
2E-17
2E-18
4E-17
MDC JiCilrnL
N/A
3E-17
6E-18
6E-17
L.L.D.+ Effluent Cone.* %Effluent
JiCilrnL 11CilmL Concentration
IE-16 9E-14 3.38E+00
1E-16 3E-14 1.66E+00
1E-16 9E-13 3.10E-02
2E-15 6E-13 3.54E+00
L.L.D.+ Effluent Cone.* %Effluent
JiCilmL 11CilrnL Concentration
JE-16 9E-14 2.78E+00
IE-16 3E-14 1.21E+00
IE-16 9E-13 2.67E-02
2E-15 6E-13 8.22E-01
L.L.D.+ Effluent Cone.* %Effluent
11CilmL 11CilrnL Concentration
IE-16 9E-14 3.31E+00
1E-16 3E-14 l.SOE+OO
IE-16 9E-13 1.71E-02
2E-15 6E-13 1.25E+00
L.L.D.+ Effluent Cone.* %Effluent
11CilmL JiCilmL Concentration
lE-16 9E-14 4.31E+00
1E-16 3E-14 3.42E-01
IE-16 9E-13 4.96E-03
2E-15 6E-13 4.88E+00
Page 7 of22
EN:RGY
·, -t • _I• I
www.enerRYlab.com
....,..,~ ... 1151
Helen1, MT 817-472-G711 • Billings, MT 801·735-4489 • Casper, WY 888-235-0515
Gillette, WY 816-181-7175 • Rapid City, SD 181·112-1225 • Collage Station, TX 888-680-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Air 2013
Lab ID: c 1401 0034-003
Client Sample ID: BHV-4
Analyses
TRACE METALS ·IN AIR
Uranium
Uranium, Activity
RADIONUCLIDES · IN AIR
Lead 210
Lead 210 precision(±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
RADIONUCLIDES • IN AIR · PER FILTER
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Uranium, Activity
Report
Definitions:
RL -Analyte reporting limit.
QCL-Quality control limit.
Result Units
5.7E-09 mg/L
3.9E-15 uCi/mL
2.9E-14 uCi/mL
3.0E-16 uCi/mL
6.1E-17 uCi/mL
4.5E-17 uCi/mL
9.0E-18 uCilmL
6.1E-18 uCilmL
1.0E-16 uCilmL
3.6E-17 uCilmL
2.6E-17 uCilmL
3920 pCiiFilter
39.6 pCiiFilter
8.2 pCiiFilter
6.0 pCiiFilter
1.2 pCiiFilter
0.81 pCi/Filter
13.8 pCi/Filter
4.9 pCiiFiiter
3.5 pCiiFilter
520 pCi/Filter
MDC -Minimum detectable concentration
Qualifiers
MCLI
RL OCL
1.5E-10
1.0E-16
0.20
Report Date: 02/06/14
Collection Date: 12/30/13
DateReceived: 01/03/14
Matrix: Filter
Method Analysis Date I By
SW6020 01/10/14 00:51 I elm
SW6020 01/10/1400:51 /elm
E909.0 01/23/14 00:40 I eli-cs
E909.0 01/23/14 00:40 I eli-cs
E909.0 01/23/14 00:40 I eli-cs
E903.0 01/20114 06:50 I imc
E903.0 01120114 06:50 I lmc
E903.0 01120114 06:50 I imc
E908.0 0111411412:00/dmf
E908.0 0111411412:00 I dmf
E908.0 01114114 12:00 I dmf
RADCALC 02/01/1413:02 I sec
RADCALC 0210111413:02 I sec
RADCALC 02/01114 13:02 I sec
RADCALC 0210111413:02 I sec
RADCALC 02/01114 13:02 I sec
RADCALC 02/0111413:02 I sec
RADCALC 02/0111413:02 I sec
RADCALC 02/01114 13:02 I sec
RADCALC 02/01/1413:02 I sec
RADCALC 02/01114 13:02 I sec
MCL-Maximum contaminant level.
NO-Not detected at the reporting limit.
Page 8 of22
EI\ERGY
••• , .. 1 •
www.energylab.com
_,.~sa.IJJZ
Helena, MT 877-472-0711 • Billings, MT BDD-735-4489 • Casper, WY 888-235-0515
Gillette, WY 111-181-7175 • Rapid City, SO 888·172-1225 • College Station, TX 181-690·2218
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: February 6, 2014
PROJECT: 4th Quarter Air 2013
SAMPLE ID: BHV-5
Quarter/Date Sampled Concentration
Air Volume Radionuclide J.!CilmL
Cl3040210-004 natu 6.66E-15
First Quarter 2013 23'Th 1.48E-15
Air Volume in mLs 226Ra 1.12E-15
1.35E+ll 210Pb l.SOE-14
Quarter/Date Sampled Concentration
Air Volume Radionuclide J.!CilmL
c 13070231-004 natu 7.35E-15
Second Quarter 2013 23oTh 1.72E-15
Air Volume in mL~ 226Ra 2.02E-15
1.37E+ II 210Pb 6.67E-15
Quarter/Date Sampled Concentration
Air Volume Radionuclide J.!CilmL
Cl3I00250-004 nalu 2.78E-15
Third Quarter 20 13 23oTh 6.92E-16
Air Volume in mLs 226Ra 3.29E-16
1.35E+ll 210Ph 6.62E-!5
Quarter/Date Sampled Concentration
Air Volume Radionuclide JJCilmL
c 140 10034-004 natu 6.70E-15
Fourth Quarter 2013 230Th 3.93E-16
Air Volume in mLs 226Ra 2.53E-16
1.34E+ll 210Pb 2.78E-14
+LLD's are from NRC Reg. Guide 4.14
Counting
Precision
J.!CilmL
N/A
3E-16
3E-17
2E-16
Counting
Precision
J.!CilmL
N/A
2E-16
4E-17
IE-16
Counting
Precision
J.!CilmL
N/A
SE-17
2E-17
!E-16
Counting
Precision
J.!CilmL
N/A
IE-16
2E-17
3E-l6
*Effluent Concentration from the NEW 10 CFR Part 20-Appendix B -Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-21 0
--
MDCJ.!CilmL
N/A
4E-17
4E-18
SE-17
MDCJ.!CilmL
N/A
2E-17
3E-18
6E-17
MDCJ.!CilmL
N/A
3E-18
2E-18
4E-17
MDCJ.!CilmL
N/A
SE-17
SE-18
6E-17
•
L.L.D.+ Effluent Cone.* %Effluent
J.!CilmL J.!CilmL Concentration
IE-16 9E-14 7.40E+00
IE-16 3E-14 4.95E+00
IE-16 9E-13 1.24E-Ol
2E-15 6E-13 3.00E+00
L.L.D.+ Effluent Cone.* %Effluent
J.!CilmL JJCilmL Concentration
!E-16 9E-14 8.16E+00
lE-16 3E-14 5.74E+00
lE-16 9E-13 2.25E-Ol
2E-15 6E-13 l.llE+OO
L.L.D! Effluent Cone.* %Effluent
J.!CilmL J.!CilmL Concentration
IE-16 9E-14 3.09E+00
lE-16 3E-14 2.31E+00
IE-16 9E-!3 3.65E-02
2E-15 6E-13 l.lOE+OO
L.L.D! Effluent Cone.* %Effluent
J.!CilmL J.!CilmL Concentration
1E-16 9E-14 7.44E+00
IE-16 3E-14 1.31E+00
IE-16 9E-13 2.81E-02
2E-15 6E-13 4.64E+00
Page 9 of 22
www.energylab.com
lill/flal Elalllra .. ,.
Helen•, MT 177-412-11711 • Billings, MT 801-735-4419 • Casper, WY 881-235-11515
Glllatta, WY 116-181-7115 • Rapid City, SD 188-172-1225 • College Station, TX 881-690-2218
LABORATORY ANAL VTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Air 2013
Lab ID: C1401 0034-004
Client Sample ID: BHV-5
Analyses
TRACE METALS -IN AIR
Uranium
Uranium, Activity
RADIONUCLIDES • IN AIR
Lead 210
Lead 210 precision(±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
RADIONUCLIDES-IN AIR· PER FIL TEA
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Uranium, Activity
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
9.9E-09 mg/L
6.7E-15 uCi/mL
2.8E-14 uCi/mL
2.9E-16 uCi/mL
6.0E-17 uCil mL
2.5E-16 uCi/mL
1.8E-17 uCi/mL
4.9E-18 uCilmL
3.9E-16 uCi/mL
1.1E-16 uCi/mL
5.5E-17 uCil mL
3730 pCi/Filter
38.3 pCi/Filter
8.0 pCiiFilter
33.9 pCi/Filter
2.4 pCi/Filter
0.66 pCi/Filter
52.7 pCiiFilter
14.1 pCiiFilter
7.4 pCiiFilter
897 pCi/Filter
MDC -Minimum detectable concentration
Qualifiers
MCL/
RL QCL
1.5E-10
1.0E-16
0.20
Report Date: 02/06/14
Collection Date: 12/30/13
Date Received: 01/03/14
Matrix: Filter
Method Analysis Date I By
SW6020 01/10/14 01 :16/ elm
SW6020 01/10/14 01:16/clm
E909.0 01/23/14 01:49/ eli-cs
E909.0 01/23/14 01:49/ eli-cs
E909.0 01123114 01 :49/ eli-cs
E903.0 01/20/14 06:50 /lmc
E903.0 01/20/14 06:50 /lmc
E903.0 01/20/14 06:50 /lmc
E908.0 01/1411412:00/dmf
E908.0 0111411412:00idmf
E908.0 01/14/1412:00 I dmt
RADCALC 02/01/14 13:02/ sec
RADCALC 02/01/14 13:02/ sec
RADCALC 02101/14 13:02 I sec
RADCALC 02/01/1413:021sec
RADCALC 0210111413:02/ sec
RADCALC 0210111413:02/ sec
RADCALC 0210111413:02 I sec
RADCALC 02101/14 13:02 I sec
RADCALC 02/01114 13:02 I sec
RADCALC 02101114 13:02 I sec
MCL-Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 10 of 22
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~£.alMa Slice IISZ
Helena, MT 877-472-0711 • Billings, MT 800-735-44119 • Casper, WY 888-235-0515
Gillette, WY 818-&8&-7115 • Rapid City, SD 888·672-1225 • College Station, TX 888-690·2218
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: February 6, 2014
PROJECT: 4th Quarter Air 2013
SAMPLE ID: BHV-6
Quarter/Date Sampled Concentration Radionuclide Air Volume f.ICi/mL
c 13040210-005 natu 4.52E-15
First Quarter 2013 2JoTh 7.93E-16
Air Volume in rnLs 226Ra 4.9!E-16
1.35E+ll 21Dpb 1.70E-14
Quarter/Date Sampled Concentration Radionuclide Air Volume f.ICilmL
c 13070231-005 "''U 5.91E-15
Second Quarter 2013 23oTh 6.74E-16
Air Volume in rnLs 226Ra 7.85E-16
1.37E+ 11 210Pb 5.18E-15
Quarter/Date Sampled Concentration Radionuclide Air Volume f.ICilmL
c 13100250-005 nalu 2.68E-15
Third Quarter 20 13 230Th 3.97E-l6
Air Volume in mL~ 226Ra 1.04E-16
1.35E+11 210Pb 6.13E-15
Quarter/Date Sampled Concentration Radionuclide Air Volume f.ICilmL
c 1401 0034-005 natu 1.60E-14
Fourth Quarter 2013 230Th 2.48E-16
Air Volume in rnLs zz6Ra 1.05E-16
1.34E+ll zwPb 2.67E-14
+LLD's are from NRC Reg. Guide 4.14
Counting
Precision
fJCi/mL
N/A
2E-16
2E-17
2E-16
Counting
Precision
f.ICilmL
N/A
9E-17
2E-17
IE-16
Counting
Precision
f.ICilmL
N/A
1E-16
IE-17
1E-16
Counting
Precision
fJCilmL
N/A
8E-17
1E-17
3E-16
*Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
DayforLead-210
•
MDC fJCi/mL
N/A
4E-17
4E-18
6E-17
MDC f.ICilmL
N/A
2E-17
3E-18
6E-17
MDCf.ICilmL
N/A
4E-17
2E-18
4E-17
MDCfJCilmL
N/A
6E-17
5E-18
6E-17
L.L.D.+ Effluent Cone.* %Effluent
f.ICilmL f.ICilmL Concentration
IE-16 9E-14 5.02E+00
IE-16 3E-14 2.64E+00
IE-16 9E-13 5.46E-02
2E-15 6E-13 2.83E+00
L.L.D.+ Effluent Cone.* %Effluent
f.ICi/mL f.ICilmL Concentration
IE-16 9E-14 6.57E+00
1E-16 3E-14 2.25E+00
lE-16 9E-13 8.73E-02
2E-15 6E-13 8.64E-Ol
L.L.D! Effluent Cone.* %Effluent
f.ICilmL f.ICi/mL Concentration
lE-16 9E-14 2.97E+00
IE-16 3E-14 1.32E+00
IE-16 9E-13 1.16E-02
2E-15 6E-13 1.02E+00
L.L.D.+ Effluent Cone.* %Effluent
f.ICilmL f.ICilmL Concentration
1E-16 9E-14 1.78E+01
IE-16 3E-14 8.26E-Ol
1E-16 9E-13 1.16E-02
2E-15 6E-13 4.44E+00
Page 11 of 22
www.energyleb.com
,.,..~_..,.
Helene, MT 817-412-0711 • Billings, MT 801-735-4489 • Casper, WV 881-235-0515
Gilleth, WV 81&-188-7115 • Rapid City, SD 888-172-1225 • Collage Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Air 2013
LabiD: c 1401 0034-005
Client Sample ID: BHV-6
Analyses
TRACE METALS -IN AIR
Uranium
Uranium, Activity
RADIONUCLIDES -IN AIR
Lead 21 o
Lead 210 precision(±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
RADIONUCLIDES-IN AIR · PER FIL TEA
Lead 210
Lead 210 precision(±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Uranium, Activity
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
2.4E-08 mgiL
1.6E-14 uCilmL
2.7E-14 uCilmL
2.8E-16 uCilmL
6.0E-17 uCilmL
1.0E-16 uCilmL
1.2E-17 uCilmL
5.2E-18 uCilmL
2.5E-16 uCilmL
8.5E-17 uCilmL
6.0E-17 uCilmL
3570 pCiiFilter
37.6 pCiiFilter
8.1 pCi/Filter
14.0 pCiiFilter
1.6 pCi/Filter
0.69 pCiiFilter
33.2 pCi/Filter
11.3 pCiiFilter
8.1 pCiiFilter
2150 pCiiFilter
MDC -Minimum detectable concentration
Qualifiers
MCL/
RL QCL
1.5E-10
1.0E-16
0.20
Report Date: 02/06/14
Collection Date: 12/30/13
Date Received: 01/03/14
Matrix: Filter
Method Analysis Date I By
SW6020 01110114 01:19 1 elm
SW6020 01110114 01 :19 1 elm
E909.0 0112311 4 02:58 1 eli-cs
E909.0 01123114 02:581 eli-cs
E909.0 01123114 02:581 eli-cs
E903.0 01120114 06:50 lime
E903.0 01120114 06:50 l ime
E903.0 01120114 06:50 l ime
E908.0 01 114114 12:00 I dmf
E908.0 01114114 12:00 I dmf
E908.0 0111411412:001dmf
RADCALC 0210111413:02 I sec
RADCALC 02101 11413:02 I sec
RADCALC 02/01114 13:021 sec
RADCALC 02101114 13:021 sec
RADCALC 0210111413:021sec
RADCALC 02101 114 13:02 I sec
RADCALC 02101114 13:02 1 sec
RADCALC 02101114 13:021 sec
RADCALC 02101 114 13:02 I sec
RADCALC 02101114 13:02 1 sec
MCL-Maximum contaminant level.
ND-Not detected at the reporting limit.
Page 12 of 22
www.enerutab.com
Alll/tfla/r...... SilaiiU
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 888-235-0515
Gillette, WY 8&&-&88-7175 • Rapid City, SO 888-&72-1225 • College Station, 1X 888-890-2218
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: February 6, 2014
PROJECT: 4th Quarter Air 2013
SAMPLE ID: Blank
Quarter/Date Sampled Concentration
Air Volume Radionuclide J!CilmL
C13040210-006 nalu 9.60E-18
First Quarter 2013 z3oTh 3.27E-18
Air Volume in mL~ 226Ra 3.89E-18
1.36E+ll 21opb -4.09E-17
Counting
Precision
J!Ci/mL
N/A
3E-18
3E-18
3E-17
Note: Thts sampl~ uses 136,000 000 L of atr volume for comparrson purposes. '
Quarter/Date Sampled Concentration Counting
Air Volume Radionuclide J!Ci/mL Precision
J!Ci/mL
C13070231-006 natu 7.23E-18 N/A
Second Quarter 2013 230Th 7.06E-18 2E-18
Air Volume in mLs 226Ra 4.52E-18 2E-18
1.36E+11 210Pb -7.38E-18 4E-17
Note: This sample uses 136,00(),000 L of air volume for Cllmparison t>nrpo$e.~.
Quarter/Date Sampled Concentration Counting
Radionuclide Precision Air Volume J!CilmL J!CilmL
c 131 00250-006 nalu 9.41E-18 N/A
Third Quarter 2013 23<Th 5.84E-18 SE-18
Air Volume in mLs 226Ra 3.64E-l8 2E-18
1.36E+ll zroPb 1.34E-18 3E-17
Note· Thts sample uses 136 000 000 L of atr volume for comparison t>urposes ' ' '
Quarter/Date Sampled Concentration Counting
Radionuclide Precision Air Volume J!CilmL J!CilmL
c 14010034-006 ni:ltu 1.79E-17 N/A
Fourth Quarter 2013 23DTh 2.83E-18 IE-18
Air Volume in mLs 226Ra 3.26E-18 2E-18
1.36E+l I zwPb 6.38E-l8 3E-17
Note: Thts sample uses 136,000,000 L of atr volume for companson purposes.
+llD's are from NRC Reg. Guide 4.14
*Effluent Concentration from the NEW I 0 CFR Part 20 -Appendix B -Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDCJ!CilmL
N/A
6E-18
4E-18
SE-17
MDCJ!CilmL
N/A
2E-18
3E-18
6E-17
MDCJ!CilmL
N/A
7E-18
2E-18
4E-17
MDCJ!CilmL
N/A
2E-18
3E-18
4E-17
L.L.D.+ Effluent Cone.* %Effluent
11CilmL J!CilmL Concentration
IE-16 9E-14 1.07E-02
IE-16 3E-14 1.09E-02
1E-16 9E-13 4.32E-04
2E-15 6E-13 -6.82E-03
L.L.D.+ Effluent Cone.* %Effluent
J!Ci/mL 11CilmL Concentration
IE-16 9E-14 8.03E-03
1E-16 3E-14 2.35E-02
1E-16 9E-13 5.02E-04
2E-15 6E-13 -1.23E-03
L.L.D! Effluent Cone.* %Effluent
J!CilmL J!CilmL Concentration
lE-16 9E-14 l.OSE-02
IE-16 3E-14 1.95E-02
IE-16 9E-13 4.05E-04
2E-15 6E-13 2.23E-04
L.L.D! Effluent Cone.* %Effluent
J!CilmL J!CilmL Concentration
IE-16 9E-14 1.99E-02
lE-16 3E-14 9.42E-03
lE-16 9E-13 3.62E-04
2E-15 6E-13 1.06E-03
Page 13 of 22
EI\ERGY
• ' 1 ,, .1 .... 1'
www.energylab.com ,.,..&alia ... 11/U
Helena, MT 877-472-0711 • Billings, MT 801-135-448tl • Casper, WY 881-235-8515
Glllatta, WY 18&-881-7175 • Rapid Ctty, SD IIB-112-1225 • College Station, TX 888-&90-2211
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Air 2013
LabiD: c 1401 0034-006
Client Sample ID: Blank
Analyses Result Units
TRACE METALS -IN AIR
Uranium 0.0036 mg/L
Uranium, Activity 2.4E-09 uCi/mL
-Air data for this sample uses a system default volume of 1 ,000 mL.
RADIONUCLIDES -IN Alij
Lead 210 8.7E-10 uCi/mL
Lead 210 precision(±) 3.5E-09 uCilmL
Lead 210 MDC 5.8E-09 uCilmL
Radium 226 4.4E-10 uCilmL
Radium 226 precision (±) 3.4E-10 uCilmL
Radium 226 MDC 4.5E-10 uCi/mL
Thorium 230 3.8E-10 uCilmL
Thorium 230 precision (±) 2.0E-10 uCilmL
Thorium 230 MDC 2.5E-10 uCilmL
-Air data for this sample uses a system default volume of 1 ,000 ml.
RADIONUCLIDES -IN AIR -PER FILTER
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Uranium, Activity
Report
Definitions:
RL -Analyte reporting limit.
QCL-Quality control limit.
0.87 pCiiFilter
3.5 pCiiFilter
5.8 pCiiFilter
0.44 pCiiFilter
0.34 pCiiFilter
0.45 pCiiFilter
0.38 pCiiFilter
0.20 pCiiFilter
0.25 pCiiFilter
2.4 pCiiFilter
MDC -Minimum detectable concentration
Qualifiers
D
D
u
u
u
u
U -Not detected at minimum detectable concentration
MCL/
RL CCL
0.000043
2.9E-11
0.20
Report Date: 02/06/14
Collection Date: 12/30/13
Date Received: 01/03/14
Matrix: Filter
Method Analysis Date I By
SW6020 01/10/14 01:22/ elm
SW6020 01 /1 0/14 01 :22 I elm
E909.0 01 /23/14 06:261 eli-cs
E909.0 01123114 06:261 eli-cs
E909.0 01123114 06:26 1 eli-cs
E903.0 01 /20114 06:50 lime
E903.0 01120114 06:50 lime
E903.0 01 120114 06:50 I imc
E908.0 01114114 12:00 I dmf
E908.0 01114114 12:00 I dmt
E908.0 01/1411412:00idmf
RADCALC 0210111413:021 sec
RADCALC 0210111413:021 sec
RADCALC 02/01114 13:021 sec
RADCALC 0210111 4 13:02 1 sec
RADCALC 0210111413:021 sec
RADCALC 02101114 13:021 sec
RADCALC 02101114 13:021 sec
RADCALC 02/0111413:021 sec
RADCALC 02/01114 13:021 sec
RADCALC 02101114 13:021 sec
MCL-Maximum contaminant level.
NO-Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 14 of 22
EI'ERGY
' I• <I •I•
Helena, MT 871-472-0711 • Billings, MT 800·735-4489 • Casper, WY 881-235-0515
Gillatta, WY 815-188-7115 • Rapid City, SD 888-172-1225 • Collage Station, TX 888-&ID-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Air 2013
Analyte Count Result
Method: E903.0
Units
Sample 10: C14010038-001AMS
Radium 226
Sample Matrix Spike
Sample 10: C14010038-002AOUP
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Sample 10: LCS-40245
Radium 226
Sample 10: MB-40245
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Qualifiers:
RL-Analyte reporting limit.
3
3
MDC-Minimum detectable concentration
1.72E-05 pCi/L
Sample Duplicate
7.12E-08 pCi/L
6.47E-08 pCi/L
9.11E-08 pCi/L
Laboratory Control Sample
24.3 pCi/L
Method Blank
0.01 pCi/L
0.2 pCi/L
0.3 pCi/L
Report Date: 02/06/14
Work Order: C1401 0034
RL %REC Low Limit High Limit RPO RPOLimlt Qual
75
113
Run: BERTHOLD 770-2_140110A
70 130
Run: BERTHOLD 770-2_140110A
37
Run: BERTHOLD 770-2_14011 OA
80 120
Run: BERTHOLD 770-2_14011 OA
NO -Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Batch: RA226·7026
01/20/14 06:50
01/20/14 08:27
209 u
01/20/14 08:27
01/20/14 08:27
u
Page 15 of 22
EI\ERGY
• } . ~. l • , II :_,
www.energylab.com
AMI/IIai.E.alllcll.lllluiiJI
Helena, MT 877-472-0711 • Billings, MT 800-735-4488 • Caspar, WY 881-235-8515
Gillette, WY 811-188· 7175 • Rapid City, SD 818-172-1225 • Collage Station, 1X 881-&10-2218
QAJQC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Air 2013
Analyte Count Result Units
Method: E908.0
Sample 10: C14010038·003AMS
Thorium 230
Sample 10: C14010038·003AMSO
Thorium 230
Sample 10: LCS-40245
Thorium 230
Sample 10: MB-40245
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Qualifiers:
RL -Analyte reporting limit.
3
MDC -Minimum detectable concentration
Sample Matrix Spike
1.1 9E-05 pCi/L
Sample Matrix Spike Duplicate
1.13E-05 pCi/L
Laboratory Control Sample
18.3 pCi/L
Method Blank
0.09 pCi/L
0.09 pCi/L
0.1 pCi/L
Report Date: 02/06/14
Work Order: C1401 0034
RL %REC Low Limit High Limit RPO RPOLimit Qual
Run : ALPHANALYST_140108B
103 70 130
Run : ALPHANAL YST_1401 08B
98 70 130 5.4
Run : ALPHANAL YST _1401 08B
101 80 120
Run : ALPHANAL YST _1401 08B
NO-Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Batch: 40245
01 /14/14 12:00
01/1411412:00
29.6
01/14/1412:00
01/14/14 12:00
u
Page 16 of 22
EN:RGY
'., ,.·1 _J''•
www.energylab.com
Mll!flal Elalflll:w SiD IBZ
Helene, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 881-235-0515
Gillatte, WY 81&-IB&-7175 • Rapid City, SD 818-172-1225 • College Station, TX 881-&90-2218
QAJQC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Air 2013
Analyte
Method: E909.0
Sample ID: LCS-20358
Lead 210
Sample ID: MB-20358
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Sample ID: C14010034-005AMS
Lead 210
Sample ID: C14010034-005AMSD
Lead 210
Qualifiers:
RL-Analyte reporting limit.
Count Result Units
Laboratory Control Sample
121 pCi/L
3 Method Blank
-0.4
3
6
pCI/L
pCI/L
pCI/L
Sample Matrix Spike
3.13E-05 pCi/L
Sample Matrix Spike Duplicate
3.15E-05 pCi/L
MDC-Minimum detectable concentration
Report Date: 02/06/14
Work Order: C14010034
RL %REC Low Limit High Limit
Run: SUB-T55050
92 80 120
Run: SUB-T55050
Run: SUB-T55050
94 70 130
Run: SUB-T55050
101 70 130
NO -Not detected at the reporting limit.
RPD RPDLimit Qual
0.9
Batch: T _20358
01/22/14 20:02
01/22/14 21 :11
u
01/23/14 04:08
01/23/14 05:17
13.8
U -Not detected at minimum detectable concentration
Page 17 of 22
EI\ERGY
• '·' >! .II• •
www.energylab.com
... Elalllcls.t rm
Helena, MT 877-472-G711 • Billings, MT BGD-735·4489 • Casper, WY 881-235-1515
Gillette, WY 816-188-7175 • Rapid City, SD 816-172-1225 • College Station, TX 881-690-2218
QAJQC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Air 2013
Analyte Count Result
Method: SW6020
Units RL %REC Low Limit
Report Date: 02/06/14
Work Order: C14010034
High Limit RPD RPDLimit Qual
Analytical Run: ICPMS2-C_140109A
Sample ID: ICV Initial Calibration Verification Standard 01/09/1413:55
Uranium 0.0494 mg/L
Sample ID: ICSA Interference Check Sample A
Uranium 1.76E·05 mg/L
Sample ID: ICSAB Interference Check Sample AB
Uranium 2.80E-06 mg/L
Method: SW6020
Sample ID: MB-40245 Method Blank
Uranium ND mg/L
Sample ID: LCS2-40245 Laboratory Control Sample
Uranium 0.0960 mg/L
Sample ID: C1401 0034-003AMS Sample Matrix Spike
Uranium 8.34E-09 mg/L
Sample ID: C1401 0034-003AMSD Sample Matrix Spike Duplicate
Uranium 8.34E-09 mg/L
Sample ID: C14010038-001 ADIL Serial Dilution
Uranium 1.60E-10 mg/L
Method: SW6020
Sample ID: MB-40245 Method Blank
Uranium ND mg/L
Sample ID: LCS2-40245 Laboratory Control Sample
Uranium 0.0997 mg/L
Sample ID: C1401 0034-00SADIL Serial Dilution
Uranium 2.16E-08 mg/L
Sample ID: C1401 0034-00SAMS Sample Matrix Spike
Uranium 2.63E-08 mg/L
Sample ID: C1401 0034-00SAM SO Sample Matrix Spike Duplicate
Uranium 2.65E-08 mg/L
Qualifiers:
RL -Analyte reporting limit.
ND -Not detected at the reporting limit.
0.00030 99 90 110
01/09/1413:58
0.00030
01/09/14 14:01
0.00030
Batch: 40245
Run: ICPMS2-C_140109A 01/1 0/14 00:35
4E-05
Run: ICPMS2-C_140109A 01/10/14 00:38
4.3E-05 96 85 115
Run: ICPMS2-C_140109A 01/10/14 00:54
1.5E-10 104 75 125
Run: ICPMS2-C_140109A 01/10/14 00:57
1.5E-10 104 75 125 0.0 20
Run: ICPMS2-C_140109A 01/1 0/14 01 :28
1.5E-10 20 N
Batch: 40245
Run: ICPMS4-C_140203A 02/04/14 00:13
4.0E-05
Run: ICPMS4-C_140203A 02/04/14 00:17
4.3E-05 100 85 115
Run: ICPMS4-C_140203A 02/04/14 00:25
1.5E-10 8.3 20
Run: ICPMS4-C_140203A 02/04/14 00:29
1.5E-10 75 125 A
Run: ICPMS4-C _140203A 02/04/14 00:33
1.5E-10 75 125 0.9 20 A
A -The analyte level was greater than four times the spike level. In
accordance with the method % recovery is not calculated.
MDC -Minimum detectable concentration
Page 18 of 22
EN:RGY . ' ... -·•
www.energylab.com
~~SM I§t
Helena, MT 877-472.0711 • Billings, MT BOD-735-448!1 • Casper, WY 811-235-8515
Gillette, WY 816-188-7175 • Rapid City, SD 818-172-1225 • College Station, TX 811-610-2218
Workorder Receipt Checklist
Energy Fuels Resources (USA) Inc
Login completed by: Debra Williams
Reviewed by: Kathy Hamre
Reviewed Date: 1/6/2014
Shipping container/cooler in good condition?
Custody seals intact on all shipping container(s)/cooler(s)?
Custody seals intact on all sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
(Exclude analyses that are considered field parameters
such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.)
Temp Blank received in all shipping container(s)/cooler(s)?
Container/Temp Blank temperature:
Water-VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Yes 0
Yes 0
Yes D
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes D
NA°C NA
Yes D
Yes D
C14010034
Date Received: 1/3/2014
Received by: dw
Carrier NDA
name:
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
Not Present D
Not Present D
Not Present 0
Not Applicable 0
No VOA vials submitted 0
Not Applicable 0
------------·-------------------------------------------------------------------·
Standard Reporting Procedures:
Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as
pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time.
Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected,
data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried
and ground prior to sample analysis.
Contact and Corrective Action Comments:
None
Page 19 of 22
E""t.r!)f ~ .... e.~S
Samples Shipped to:-=E~n~er~g~y ..:;.La:::.;b:-:· 9:.;.;ra~to~r~ie:.::s ________ Contact: Garrin Palmer
2393 Salt Creek Hwy Ph: 435 678 4.115
Casper WY, e2601 gpa!mar@energyfuels.~
Chain of Custody/Sampling Analysis Request
ProJect
4th Quarter Air 2013
SamplefD Date Collected
BHV·1 1/10/13-12/30/13
BHV-2 1/10/13-12/30/13
BHV-4 1/10i13-12/30/13
BHV-5 1/10/13-12/30/13
BHV-6 1/10/13-12/30/13
Blank 1/10/13-12/30/13
Comments:
Relinquished By:(Signature)
Garrin Palmer 1 . ;;.............::. p~
Relinquished By:( Signature)
Samplers Name Samplers Signature
Garrin Palmer I&~ o.L ...
Time
COllected laboretorv Analysis Requested
NA U-NAT. Th-230 Ra-226, Pb-210
NA U-NAT, Th-230, Ra-226, Pb-210
NA U-NAT, Th-230, Ra-226, Pb-210
NA U-NAT, Th-230, R&-226, Pb-210
NA U-NAT, Th-230, Ra-226, Pb-210
NA U-NAT, Th-23Q,_Ra-226, Pb-210
Date/Time Received By:(Signature)
12/30/2013
1200
Pate/Time
Page 20 of22
ATTACHMENT D
AIR PARTICULATE LOADING GRAPHS AND SUPPORTING DATA
0 0 0 9 ....
0 0 0 .... 0
0 0 0 0 .... 0 0 .... 0 0 .... 0 0 0 0
1/5/2009
3/5/2009
5/5/2009
7/5/2009
9/5/2009
11/5/2009
1/5/2010
3/5/2010 l>
+ -· 5/5/2010 .,
~ OJ " :I: 7/5/2010 OJ < " I .... -· 9/5/2010 0
+ ~
11/5/2010 -g OJ OJ :I: ., < 1/5/2011 -I " N -· 3/5/2011 n
+ c -5/5/2011 · OJ OJ " :I: t1) < I 7/5/2011 r-~
0
+ 9/5/2011 OJ c. -· OJ 11/5/2011 ~ :I: < OQ I ll1 1/5/2012 -
+ 3 3/5/2012 OQ ........ OJ 3 :I: 5/5/2012 < I w en
7/5/2012 -
9/5/2012
11/5/2012
1/5/2013
3/5/2013
5/5/2013
7/5/2013
9/5/2013
11/5/2013
0 0 !=' ......
0 0 ...... 0
0 ...... 0 0 ...... 0 0 0 0 0 0 0
1/5/2009 ..;
3/5/2009
5/5/2009
7/5/2009
9/5/2009
11/5/2009
1/5/2010
3/5/2010
5/5/2010 ~ T ~ J I "' :::t
7/5/2010 -1 I ___.,.. I I < I
9/5/20101 I _#<Z I I ~
""C
11/5/2010 -1 .........r'! ... I I QJ .., ,...
1/5/2011 -l ... .,..........., •I I I -· n c
3/S/2011 j -
f_2£j; -
+
QJ • ,...
OJ 5/5/2011 tt)
::r: • r-< 7/5/2011 0 I ...... QJ
9/5/2011 -l ~ I I c. -:::s
11/5/2011 -l • -:1 • I I (JQ • -1/5/2012 -1 • I I 3
(JQ
3/5/2012 -1 1 ~. I • I I ......... -3
5/5/2012 -1 r ~ ... I • I w -
7/5/2012
9/5/2012
11/5/2012
1/5/2013
3/5/2013
5/5/2013
7/5/2013
9/5/2013
11/5/2013
0 0 ~ ......
0 0 ...... 0 0 ...... 0 0 ...... 0 0 0 0 0 0 0
1/5/2009
3/5/2009 -
5/5/2009
7/5/2009
9/5/2009
11/5/2009
1/5/2010
3/5/2010
5/5/2010 ~ -~-• ~ J I -~· "' ::I:
7/5/2010 -1 I -ll:li I ! < I
9/5/2010 -1 I • ~ .. I I N
""0
11/5/2010 -1 ~~ "i I I aJ .., ....
1/5/2011 -l ~ -I I -· --• n c:
3/5/2011 j -
+ aJ ....
c:J 5/5/2011 tD
::r: r-< I 7/5/2011 0 N aJ
9/5/2011 -j I• .... -I I c.. --::::J
11/5/2011 -1 ·--~ • I I OQ -1/5/2012 -1 .r: = • I I 3 OQ
3/5/2012 -1 ~I • .... I I "" • 3
5/5/2012 -1 I -~ I I w -
7/5/2012
9/5/2012
11/5/2012
1/5/2013 "
3/5/2013
5/5/2013 .
7/5/2013
9/5/2013
11/5/2013
0 0 0 !=' ~
0 0 0 ~ 0 0 0 ~ 0 0 0 ~ 0 0 0 ~ 0 0 0 0
1/5/2009
3/5/2009
5/5/2009
7/5/2009
9/5/2009
11/5/2009
1/5/2010
3/5/2010
5/5/2010 ~ I -1-.S-. L I D'
:I:
7/5/2010 1 I *""
. -......,..--I I < ...
I
9/5/2010 1 I I I ~
""C
11/5/20101 I F I I QJ
""' ,...
1/5/2011 1 I • b r ' I -· -n
r::::
3/S/2011 j -
+
QJ ,...
OJ 5/5/2011 t1)
I r-< 7/5/2011 0 I ~ QJ
9/5/2011 -j I ~ ~ I I a. -::::s
11/5/2011 -l -I , 1 .. ~ I I OQ ... -1/5/2012 -l I ~ .. ' • l .. I 3 -OQ
3/5/2012 -1 I IIJr _j ... I I ........
3
5/5/2012 ·I I I --...._____ I I w -
7/5/2012 .
9/5/2012
11/5/2012
1/5/2013
3/5/2013
5/5/2013
7/5/2013 .
9/5/2013 -
11/5/2013
0 0 !=> .....
0 0 ..... 0 0 ..... 0 0 ..... 0 0 0 0 0 0 0
1/5/2009
3/5/2009 -
5/5/2009
7/5/2009
9/5/2009
11/5/2009 .
1/5/2010
3/5/2010 -
5/5/2010 4 I --. ~ I_ I Ol
:::t
7/5/2010 ~ I __,.. I I < I
9/5/2010 ~ I ~ I I U1
-a
11/5/2010 -j I I QJ .., ,...
1/5/2011 -j I I -· n c:
3/5/2011 J c .. -
+ t%· QJ • ,...
!P 5/5/2011 tD
I: • r-< 7/5/2011 0 I lJ'I QJ
9/5/2011 -j ........_. ~-I I c.. -::::J
11/5/2011 -1 • r::;::::::: • ~ I OQ -1/5/2012 -1 -•I I I I 3 --OQ
3/5/2012 -1 -I ..-.,..._ -• • I I ........ ----3
5/5/2012 -l I -~~-I w -
7/5/2012
9/5/2012
11/5/2012
1/5/2013
3/5/2013 -
5/5/2013
7/5/2013
9/5/2013
11/5/2013
0 0 !=> 1-" 0 0 1-" 0 0 1-" 0 0 1-" 0 0 0 0 0 0 0
1/5/2009
3/5/2009
5/5/2009
7/5/2009
9/5/2009
11/5/2009
1/5/2010
3/5/2010
5/5/2010 -1
r· )( ~~ ..1 I .,
:I:
7/5/2010 -1 I ~""*' I I < I
9/5/2010 -1 I ~ I I en
""C
11/5/2010 1 '~ j>E .. I I DJ
)f u )( ~
1/5/2011 -l }f-:m I I -· ~ n c
+ 3/5/2011 j -DJ r+
OJ 5/5/2011 tD
::I: r-< I 7/5/2011 0 (J') .. DJ
9/5/2011 1 ~t ==-t( I I a. .. -· :::l
11/5/2011 -1 )( f?L ·Jc I I OQ )( -1/5/2012 -l " lijt= Jt I I 3 " OQ
3/5/2012 1 1~. -. )( )( I II """ 3
5/5/2012 -l r· ~ I I w -
7/5/2012
9/5/2012 -
11/5/2012
1/5/2013
3/5/2013
5/5/2013
7/5/2013
9/5/2013
11/5/2013
Period: July 2, 2013 through, October 1, 2013 (3rd Quarter 2013) Page 1
BHV-1 on stream% 100.2% BHV·1 Total Volume: 4.83E+06
Week Filter Start Stop Stop Start Total Total Loading, Per Cent
# Number Date li>lite Gross Tare Net Time Time Time Uters IJlg/_1113 OnStrllam SCFM
I 8400895 2-Jul-D 8-Jul-13 4.b081. 4.2860 0.3222 48245.1 48101.8 8598.0 8.886.591 0.0363 99.5% 36.5
2 8400889 08-Jul-13 15-Jul-13 4.5688 4.3248 0.2440 48413.6 48245.1 10112.4 10,594,997 0.0230 100.3% .n.o
3 8400878 15-Jul-13 22-Jul-13 4.5453 4.2774 0.2679 48579.7 48413.6 9967.8 10.443,497 0.0257 98.9% 37.0
4 8400876 22-Jul-13 29-Jul-13 4.7394 4.3432 0.3962 48750.1 48579.7 10218.6 10,706,266 0.0370 101.4% 37.0
5 8400868 29-Jul-13 5-Aug-13 4.5290 4.2808 0.2482 48921.9 48750.1 10308.0 10,799,9n 0.0230 102.3% 37.0
6 84008f>4 05-Aug-13 12-Aug-13 4.5488 4.3096 0.2392 49086.3 48921.9 9864.0 10.334,743 0.0231 97.9% 37.0
7 8400853 12-Aug-13 19-Aug-13 4.5623 4.3507 0.2116 49254.1 49086.3 10068.6 10,520,596 0.0201 99.9% 36.9
8 8400851 19-Aug-13 26-Aug-13 4.4989 4.3192 0.1797 49421.1 49254.1 10024.2 10.474,203 0.0172 99.4% 36.9
9 8400845 26-Aug-13 3-Sep-13 4.4437 4.2878 0.1559 49613.2 49421.1 11526.6 12,044,048 0.0129 100.1 % 36.9
10 8400835 03-Sep-13 9-Sep-13 4.5353 4.3158 0.2195 49758.3 49613.1 8708.4 9.025.356 0.0243 100.8% 36.6
ll 8400833 09-Sep-13 16-Sep-13 4.4214 4.3365 0.0849 49923.8 49758.3 9931.2 10.236,418 0.0083 98.5% 36.4
12 8400823 16-Sep-13 24-Sep-!3 4.5364 4.3208 0.2156 50092.6 49923.8 10125.6 10,436,792 0.0207 87.9% 36.4
13 8400821 24-Sep-13 1-0cL·l3 4.6607 4.2687 0.3920 -~0289.0 50092.6 11784.6 12,146,779 0.0323 116.9% 36.4
Totals 91 2184.0 4.5537077 4.309331 0.2444 131238 136'.650,219 0.0234 100.3-% 36.8
BHV-2 on stream% 100.1% BHV·2 Total Volume: 4.82E-Kl6
Week Filter Start Stop Stop Start Total Total Loading, Per Cent
N-Number Daro Date GfOSS. Tare Not Tim a Time Time Utera mg!m3 Onslroam SCFM
1 84006M-02-Jut-13 08-Jul-13 4.6184 4·.3299 0.2885 58511.1 663'67.8 8599.8 8,888,452 0.0325 99.5% 36.5
2 8400888 08-Jul-13 15-Jul-13 4.5509 4.3153 0.2356 58679.7 58511.1 10112.4 10,594,997 0.0222 100.3% 37.0
3 8400879 15-Jul-13 22-Jul-13 4.6160 4.3090 0.3070 58845.8 58679.7 9966.0 10,441,611 0.0294 98.9% 37.0
4 8400875 22-Jul-13 29-Jul-13 4.6912 4.3053 0.3859 59016.1 58845.6 10218.6 10,706,266 0.0360 101.4% 37.0
5 8400869 29-Jul-13 05-Aug-13 4.5923 4.3033 0.2890 59187.6 59016.1 10290.6 10,781,702 0.0268 102.1% 37.0
6 8400863 05-Aug-13 12-Aug-13 4.5861 4.3305 0.2556 59352.4 59187.6 9886.2 10,358,002 0.0247 98.1% 37,0
7 8400854 12-Aug-13 19-Aug-13 4.5308 4.3137 0.217t 59520.1 59352.4 10066.8 10,516,715 0.0206 99.9% 36.9
6 8400650 19-Aug-13 26-Aug-13 4.5679 4.3395 0.2284 59687.2 59520.1 10024.8 10,474,830 0.0218 99.5% 36.9
9 6400644 26-Aug-13 03-Sep-13 4.6136 4.3342 0.2794 59879.4 59687,2 11529.0 12,046,556 0.0232 100.1% 36.9
10 6400836 03-Sep-13 09-Sep-13 4.6062 4.3522 0.2540 60024.0 59679.4 8677.8 8,993,642 0.0282 1004% 36.6
11 8400832 09-Sep-13 16-SeJ}-13 4.4500 4.3524 0.0976 60189.6 60024.0 9933.6 10,238,892 0.0095 96.5% 36.4
12 6400824 16-Sep-13 24-SeJ}-13 4.4644 4.2920 0.1724 60358.2 60189.6 10It9.6 10,430,808 0.0165 87.8% 3b.4
13 8400820 241~Sep-13 01-0ct-13 4.7844 4.3165. 0.4659 60654.7 8.0358.-2 11789.4 12,151 ,726 0.0383 117.0% 36.4
Totals 91 2184.0 4.59017 4.32275 0.2674 131214.6 136.625.999 0.0254 100.3% 36.8
BHV-4 on stream % 98.8% BHV-4 Total Volume: 4.76E+06
Week Filter Start Stop Stop Start Total Total Loading, Per Cent
# Number Data Date Gross-Tare Net Time Time Time Lllers mc/m3 On·Strearn SCFM
1 6400893 02-Jul-13 08-Jul-13 4.5226 4.3486 0.1740 33790.3 33646.8 8611.2 8,900,234 0.0196 99.7% 36.5
2 8400887 08-Jul-13 15-Jul-13 4.4725 4.3197 0.1528 33955.4 33790.3 9906.6 10,379,376 0.0147 98.3% 37.0
3 8400680 15-Jul-13 22-Jul-13 4.6261 4.3046 0.3235 34119.7 33955.4 9856,8 10,327,199 0.0313 97.8% 37.0
4 8400874 22-Jul-13 29-Jul-13 4.7694 4.3361 0.4333 34289.6 34119.7 10206.0 10,693,064 0.0405 101.2% 37.0
5 8400866 29-Jul-13 05-Aug-13 4.4783 4.3207 0.1576 34461.0 34289.8 10269.0 10,759,071 0.0146 101 .9% 37.0
6 8400862 05-Aug-13 12-Aug-13 4.5603 4.2892 0,2711 34626.0 34461.0 9902.4 10,374,976 0.0261 98.2% 37.0
7 8400855 12-Aug-13 19-Aug-13 4.4868 4.2856 0.2012 34794.0 34626.0 10077.0 10,529,373 0.0191 100.0% 36.9
8 8400849 19-Aug-13 26-Aug-13 4.5790 4.3256 0.2534 34961.9 34794.0 10075.2 10,527,492 0.0241 100.0% 36.9
9 8400843 26-Aug·13 03-Sep-13 4.5364 4.3436 0.1928 35153.1 34961.9 11472.6 11,987,624 0.0161 99.6% 36.9
10 8400837 03-Sep-13 09-Sep-t3 4.5231 4.3170 0.2061 35298.7 35153.1 8735.4 9,053,339 0.0228 101.1% 36.6
11 8400831 09-Sep-13 16-Sep-t3 4.3589 4.2923 0.0666 35463.3 35298.7 9874.2 10,177,666 0.0065 96.0% 36.4
12 8400625 16-SeJ}-13 24-Sep-13 4.4342 4.2935 O.t407 35607.7 35463.3 8668.2 6,934,602 0.0157 75.2% 36.4
13 8400819 24,Sep.13 01-0ct-t3 4.62t9 4.3t01 0.3116 35805.5 35607.7 11868.0 12,2.32.7.42 0.0255 117.7% 36.4
Totals 91 2184.0 4.53627 4.31435 0.2219 129522.6 134,878.759 0.0213 99.1% 36.8
BHV-5 on stream % 96.8% BHV·5 Total Volume: 4.76E+06
Week Filter Start Stop Stop Start Total Total Loading, Per Cent
ll ·Number Oa1ec Dale Gross-Tare Net n me llTTie Time liters rng/m3 OnSirearn SCFM
1 8400892 02-Jul-13 06-Jul-13 4.6134 4.2970 0.3164 57597.2 57453.6 8599.8 6,888,452 0.0356 99.5% 36.5
2 8400886 08-Jul-13 15-Jul-13 4.5522 4.3379 0.2143 57762.3 57597.2 9907.8 10,360,633 0.0206 96.3% 37.0
3 8400881 15-Jul-13 22-Jul-13 4.5530 4.2800 0.2730 57926.3 57762.3 9842.4 10,312,112 0.0265 97.6% 37.0
4 8400873 22-Jul-13 29-Jul-13 4.6950 4.3362 0.3588 58096.8 57926.3 10226.4 10,714.438 0.0335 101.5% 37.0
5 8400866 29-Jul-13 05-Aug-13 4.5163 4.3171 0.1992 58268.0 58096.6 10275.6 10,765,966 0.0185 101.9% 37.0
6 6400661 05-Aug-13 12-Aug-t3 4.5092 4.2960 0.2112 56433.0 56266.0 9895.8 10,366,061 0.0204 98.2% 37.0
7 8400856 12-Aug-13 19-Aug-13 4.4847 4.2992 0.1855 58600.6 58433.0 10055.4 t0,506,604 0.0177 99.8% 36.9
8 8400848 19-Aug-13 26-Aug-13 4.5269 4.2649 0.2420 58768.5 58600.6 10074.0 10,526,239 0.0230 99.9% 36.9
9 8400842 26-Aug-13 03-Sep-13 4.4672 4.3183 0.1469 58959.6 58768.5 11467.2 11,961,962 0.0124 99.5% 36.9
10 6400836 03-Sep-13 09-Sep-13 4.5129 4.3295 0.1834 59105.6 58959.6 8758.8 9,077,591 0.0202 101.4% 36.6
11 6400830 09-Sep-13 16-Sep-13 4.4t96 4.3409 0.0787 59270.2 59105.6 9879.6 10,183,232 0.0077 98.0% 36.4
12 8400626 16-Sep-13 24-Sep-13 4.5131 4.3275 0.1656 59414.8 59270.2 8671.8 6,936,312 0.0208 75.3% 36.4
13 8400816 24·Sep-13 01-0ct-13 4.5715 4.2506 0.3207 59612.4 594t4.6 11857.8 12,222,229 0.0262 117.6"~ 36.4
Totals 91 2184.0 4.53346 4.30902 0.2244 129512.4 134 866,059 0.0216 99,1% 36.8
Page 21 of 22
Period: July 2, 2013 through , October 1, 2013 (3rd Quarter 2013)
BHV-6 on slream%
Week Filter Start
# Number Date
1 8400891 02,~ul-13
2 8400885 08-Jul-13
3 6400882 15-Jul-13
4 8400872 22-Jul-13
5 8400865 29-Ju\-13
6 8400860 05-Aug-13
7 8400657 12-Aug-13
8 8400847 19-Aug-13
9 8400841 26·Aug·13
10 8400839 03-Sep-13
11 8400629 09-Sep-13
12 8400627 16-Sep-13
13 8400817 24--SQp-13
Totals 91
All. BHV on stream %
Week
# Blanks
Start
Date
I 8400884 02-Jul-13
2 8400863 06-Jul-13
3 8400877 15-Jul-13
4 8400870 22-Jul-13
5 8400859 29-Jul-13
6 6400585 05-Aug-13
7 8400852 12-Aug-13
8 840084() 19-Aug-13
9 8400846 26-Aug-13
10 8400634 03-Sep-13
11 8400828 09-Sep-13
12 8400622 16-Sep-13
13 8400816 24-Sep-13
Totals 91
98.6%
Stop
Date
08-JUI·13
15-Jul-13
22-Jul-13
29-Jul-13
05-Aug-13
12-Aug-13
19-Aug-13
26·Aug-13
03-Sep-13
09-Sep-13
16-Sep-13
24-Sep-13
01-0ct-13
2164.0
99.3%
Stop
Date
OS·Jul-13
15-Jul-13
22-Jul-13
29-Jul·13
05-Aug-13
12-Aug-13
19-Aug-13
26-Aug-13
03-Sep-13
09-Sep-13
16-Sep-13
24-Sep-13
01-0ct-13
2184.0
Stop
Gross Tare Net Time
4.8363 4.3149 0.3214 5997 3
4.6593 4.3053 0.3540 6158.3
4.6970 4.3142 0.2828 6322.1
4.72_55 4.3150 0.4105 6492.5
4<5•f15 4.2685 0.2730 6663.7
4.4660 4.3251 0.1409 6828.7
4.5284 4.3214 0.2070 6996.3
4.5428 4.3321 0.2107 7164.2
4,.5013 4.3272 0.1741 7354.7
4.5028 4.3421 0.1607 7500.3
4.4 175 4.3230 0.0945 7665.1
4.5286 4.3203 0.2063 7809.6
4.5045 4.2993 0.2052 8007.0
4.54996 4.31603 0.2339
Net
4.2853
4.3314
4.3458
4.3190
4.3120
4.2671
4.3347
4.3496
4.3352
4.2951
4.2764
4.3025
4.2966
4.3116
Page2
BHV-6 Total Volume: 4.75E+06
Start Total Total Loading. Per Cent
T1mtl Time LIIDJS mll'_m3 On Stre~tm SCFM
5854.1 SSV-1.0 8,880,390 0.0362 99.4% 36.5
5997.3 9658.8 10,119,750 0.0350 95.8% 37.0
6158.3 9825.0 10,293,882 0.0275 97.5% 37.0
6322.1 10224.6 10,712,552 0.0383 101.4% 37.0
6492.5 10273.8 10,764,100 0.0254 101.9% 37.0
6663.7 9898.2 10,370,575 0.0136 98.2% 37.0
6828.7 10054.8 10,506,177 0.0197 99.6% 36.9
6996.3 10074.0 10,526,239 0.0200 99.9% 36.9
7164.2 11430.6 11,943,739 0.0146 99.2% 36.9
7354.7 8737.2 9,055,204 0.0177 101.1% ~6.6
7500.3 9890.4 10,194,364 0.0093 98.1% 36.4
7665.1 8668.8 6,935.220 0.0231 75.3% 36.4
7809.6 11845.2 12,209,241 0.0168 117.5% 36.4
129173.4 134,511,432 0.0229 98.9"k 36.8
Page.22 of 22
·N"rtod: September 30,2013 through, December 30,2013 (4th Quarter 2013) Page 1
BHV-1 en stream % 99.8% BHV-1 Total Volume: 4.76E+06
Week Filler Start Stop Stop Start Total Total loading, Per Cent
# Number Date Dale Gross Tare Net Time Time Time Uten mg/m3 On Stream SCFM
I 8400SIS f.()c!-13 8-0ct-\3 4.3972 4.2813 0.1159 50429.9 50289.0 8456.4 8,740,238 0.0133 83.9*/o 36.5
2 8400806 08.0Ct-13 14-0ct-13 4.4766 4.2905 0.1861 50597.4 50429.9 10048.2 10,527,734 0.0177 116.3!/o 37.0
3 8400803 14<01;1·13 21-0ct-13 4.4045 4.3191 0,0852 50764.2 50597.4 10011.0 10,488,758 0.0081 99.3% 37.0
4 8398997 21-0ct·ll 28-0ct-13 4.4812 4.3732 0.1 080 50931.2 50764.2 10021.2 10,499,445 0.0103 99.4% 37.0
5 8398988 28.0Ct·IJ 4-Nov-13 4.6182 4.3167 0.3015 51 101.9 50931.2 10239.6 10,728,268 0.0281 101.6% 37.0
6 8398986 04-Nov-I:J 11-Nov-ll 4.4092 4.3104 0.0988 51268.4 51101.9 9993.0 10,469,899 0.0094 99.1% 37.0
7 8398975 11-Nov-13 18-Nov-13 4.4720 4.3198 0.1522 51439.2 51268.4 10246.2 10,706,169 0.0142 101.6% 36.9
8 8398973 18-Nov-13 25-Nov-13 4.3892 4.3182 0.0710 51606.5 51439.2 10039.8 10,490,503 0.0068 99.6% 36.9
9 8398964 25-Nov-13 2-Dcc-13 4.4270 4.3568 0.0702 51773.7 51606.5 10032.6 10,482,980 0.0067 99.5% 36.9
10 8398961 02-Dec-13 9-Dcc-13 4.4582 4.3549 0.1033 51942.6 51773.7 10133.4 10,502,221 0.0098 100.5% 36.6
11 S398952 09-Dec-13 16-Dec-13 4.3863 4J228 0.0635 52112.4 51942.6 10188.6 10,501,729 0.0060 101.1% 36.4
12 8398949 16-Dec-13 23-Dec-13 4.4127 4.3345 0.0782 52276.8 52112.4 9861.0 10,164,060 0.0077 97.8% 36.4
13 8:398943 23-Dec-13 30-Dec-13 4.4170 4.3678 0.0492 52444.1 52276.3 10069.8 10,379,277 0.0047 ~9.9"/o 36.4
Totals 90 2160.0 4.442254 4.328169 0.1141 129340.8 134.681,283 0.0110 IOO.O'r. 36.8
BHV-2 on stream % 99.8% BHV-2 Total Volume: 4.75E+06
Week Filter Start Stop Stop Start Total Total Loading. Per Cent
# Number Date Date Gro.ss Tare· Net Time Tlme Titno Ul&rs I'IIQI.m3 On Stream SCFM
1 8400814 01-Qct-13 O~cl-13 .4.4947 4...2950 0.19.97 60696.1 60554.7 8484.0 8,768,765 0.0228 84.2% 36.5
2 8400807 08-0ct-13 14-0ct-13 4.5124 4.2982 0.2142 60863.5 60696.1 10045.2 10,524,590 0.0204 116.3% 37.0
3 8400802 14-0ct-13 21-0ct-13 4.4345 4.3019 0.1326 61030.8 60863.5 10034.4 10,513,275 0.0126 99.5% 37.0
4 8398996 21-0cl-13 28-0ct-13 4.5532 4.3318 0.2214 61197.4 61030.8 9997.2 10,474,300 0.0211 99.2% 37.0
5 8398989 28-0cl-13 04-Nov-13 4.6117 4.3157 0.2960 61368.0 61197.4 10238.4 10,727,011 0.0276 101.6% 31.0
6 8398985 04-Nov-13 11-Nov-13 4.5105 4.3111 0.1994 61534.6 61368.0 9995.4 10,472,414 0.0190 99.2% 37.0
7 8398976 11-Nov-13 18-Nov-13 4.4981 4.2480 0.2501 61705.1 61534.6 10231.2 10,690,495 0.0234 101.5% 36.9
8 8398972 18-Nov-13 25-Nov-13 4.3795 4.2907 0.0888 61872.7 61705.1 10056.0 10.507,430 0.0085 99.8% 36.9
9 8398965 25-Nov-13 02-Dec-13 4.3730 4.2968 0.0762 62040.0 61872.7 10035.0 10,485,488 0.0073 99.6% 36.9
10 8398960 02-Dec-13 09-Dec-13 4.5102 4.3836 0.1266 62208.8 62040.0 10131.6 10,500,356 0.0121 100.5% 36.6
11 8398953 O~Dec-13 16-Dec-13 4.4372 4.3534 0.0838 62378.4 62208.8 1017D.6 10,483,175 0.0080 100.9% 36.4
12 8398948 16-Dec-13 23-Dec-13 4.4174 4.3263 0.0911 62542.2 62378.4 9832.2 10,134,375 0.0090 97.5% 36.4
13 8398942 23-Dec-13 30-Dec-13 4.4006 4.3319 0.06&7 62710.0 62542.2 10067.4 10.376,804 0.0066 99.9% 36.4
Totals 90 2160.0 4.47f769 4.31418 0.1576 12.9318.6 134.658.,478 0.0163 100.0%, 36.8
BHV-4 on stream % 99.3% BHV-4 Total Volume; 4.73E+06
Week Alter Start Stop Stop Start Total Total loading. Per Cent
# Number Date Date Gross Tare Nat Timl!l nme Time lllers lll9Lm3 On Stream SCFM
1 8400813 Ot-Od-13 o~et-13 4.4306 4.3043 0.1263 35934.6 35805.5 7746.0 8,005,994 0.0158 76.8% 36.5
2 8400808 08-0ct-13 14-0ct-13 4.4522 4.2406 0.2116 36099.7 35934.6 9904.8 10,377,490 0.0204 114.6% 37.0
3 8400801 14-0ct-13 21-0ct-13 4.3550 4.2699 0.0851 36266.5 36099.7 10010.4 10.488.130 0.0081 99.3% 37.0
4 8398995 21-0ct-13 28-0ct-13 4.4467 4.3279 0.1188 36434.6 36266.5 10080.6 10,561,680 0.0112 1 OO.O"A. 37.0
5 8398990 28-0ct-13 04-Nov-13 4.5863 4.3415 0.2448 36604.1 36434.6 10174.2 10,659,747 0.0230 100.9% 37.0
6 8398984 04-Nov-13 11-Nov-13 4.4491 4.3476 0.1015 36770.9 36604.1 10005.0 10,482,472 0.0097 99.3% 37.0
7 8398977 11-Ncv-13 18-Nov-13 4.5076 4.3337 0.1739 36941.2 36770.9 1021 9.2 10.677,957 0.0163 101.4% 36.9
8 8398971 18-Nov-13 25-Nov-13 4.4143 4.3267 0.0876 37109.0 36941.0 10080.0 10,532,508 0.0083 100.0% 36.9
9 8398966 25-Nov-13 02-Dec-13 4.4158 4.3318 0.0840 37276.1 37109.0 10021.8 10,471.695 0.0080 99.4% 36.9
10 8398959 02-Dec-13 09-Dec-13 4.4365 4.3539 0.0826 37445.0 37276.1 10136.4 10,505,330 0.0079 100.6% 36.6
11 8398954 09-0ec-13 16-Dec-13 4.4163 4.3657 0.0496 37615.6 37445.0 10233.6 10,548,112 0.0047 101.5% 36.4
12 8398947 16-Dec-13 23-Dec-13 4.3988 4.3596 0.0392 37780.8 37615.6 9912.6 10,217,246 0.0038 98.3% 36.4
13 8398941 2.3-0ec-13 3Q.Dec-13 4.4032 4.3489 0.0543 37950.7 37780.8 10192.2 10,505.439 0.0052 101.1% 36.4
Totals 90 2160.0 4.439338 4.32708 0.1123 128716.8 134,033',800 0.0110 99.6% 36.8
BHV-5 on stream % 99.3% BHV-5 Total Volume: 4.73E+06
Week Aller Start Stop Stop Start Total Total loading, Per Cent
II -Number OaJe Date Gross Tare Net Time Time Time Utett; malm3 On Slteam SCFM
1 8400812 01-0ct-13 OB-Oct-13 4.3906 4.2658 0.1247 59741 .5 59612.4 7749.6 8,llU9,T15 0.0166 76.9% 36.5
2 8400809 08-0ct-13 14-0ct-13 4.4786 4.2751 0.2035 59906.7 59741.5 9907.8 10,380,633 0.0196 114.7% 37.0
3 8398999 14-0ct-13 21-0ct-13 4.4309 4.3364 0.0945 60073.6 59906.7 10013.4 10.491,273 0.0090 99.3% 37.0
4 8396994 21-0ct-13 28-0ct-13 4.4691 4.3497 0.1194 60241.5 60073.6 10077.6 10,558,537 0.0113 100.0% 37.0
5 8398991 21).0ct-13 04-Nov-13 4.5823 4.3488 0.2335 60411.2 60241.5 10179.0 10,664,776 0.0219 101.0% 37.0
6 8398983 04-Nov-13 11-Ncv-13 4.4468 4.3439 0.1029 60577.8 60411.2 99912 10,474,300 0.0098 99,2% 37.0
7 8398978 11-Ncv-13 18-Nov-13 4.5004 4.3340 0.1664 60747.7 60577.8 10197.0 10,654,760 0.0156 101.2% 36.9
6 8398970 18-Nov-13 25-Nov-13 4.4039 4.3309 0.0730 60915.6 60747.7 10072.2 10,524,356 0.0069 99.9% 36.9
9 8398967 25-Nov-13 02-0ec-13 4.4231 4.3521 0.0710 61082.5 60915.6 IOOIS.S 10,465,426 0.0068 99.4% 36.9
10 8398958 02-Dec-13 09-Dec-13 4.4399 4.3454 0.0945 61251 .6 61082.5 10143.0 10,512,171 0.0090 100.6% 36.6
11 8398955 09-0ec-13 11Klec-13 4.3657 4.2996 0.0661 61422.1 61251.6 10232.4 10.546,875 0.0063 101.5% 36.4
12 8398946 16-Dec-13 23-Dec-13 4.4380 4.3511 0.0869 61587.6 61422.1 9930.6 10,235,799 0.0085 98.5% 36.4
13 8398940 23-Dec-13 30-Dec-13 4.4161 4.3539 0.0622 61757.2 61587.6 ]0173.0 10.485,649 0.0059 100.9% 36.4
Tolals 90 2160.0 4.445023 4.32976 0.1153 128688.6 134.004,271 0:0112 99.5% 36.8
Page 21 of 22
... -.....
Pertod: September 30, 2013 through, December 30, 2013 (4th Quarter 2013)
BHV-6 on stream %
Week Filter Start ; Number Dale
1 13400811 01-0ct-13
2 8400810 08-oct-13
3 8398998 14-0ct-13
4 8398993 21-0ct-13
5 8398992 28-0ct-13
6 8398982 04-Nov-13
7 8398979 11-Nov-13
8 8398969 18-Nov-13
9 8398968 25-Nov-13
10 8398957 02-Dec-13
11 83989~ 09-Dec-13
12 8398945 16-Dec-13
13 8398939 23-Dec-13
Totals 90
ALL BHV on stream %
Week
/1. Blanks
Start
Date
1 8400805 01-0ct-13
2 8400804 08-0Cl·13
3 8399000 14-0ct-13
4 8398967 21-0ct-13
5 8398981 28-0ct-13
6 8398980 04-Nov-13
7 8398974 11 -Nov-13
8 8398963 18-Nov-13
9 8398962 25-Nov-13
10 8398951 02-Dec-13
11 8398950 09-Dec-13
12 8396944 16-Dec-13
13 8398933 23-.De.c-13
Totals 90
99.3%
Stop
Date
08-0ct-13
14-0ct-13
21-0ct-13
28-0ct-13
04-Nov-13
11-Nov-13
18-Nov-13
25-Nov-13
02-Dec-13
09-Dec-13
16-Dec-13
23-0ec-13
30-0ec-13
2160.0
99.5%
Stop
Date
08-0ct-13
14-0ct-13
21-0ct-13
2S-Oct-13
04-Nov-13
11-Nov-13
18-Nov-13
25-Nov-13
02-Dec-13
09-Dec-13
16-0ec-13
23-Dec-13
3Q-Dec-13
2160.0
Gross
4.3948
4.4570
4.4308
4.4780
4.5000
4.3811
4.4728
4.4145
4.4022
4.4715
4.4133
4.3937
4.3385
4.43'0669
Net
4.2n3
4.2850
4.3485
4.3375
4.3339
4.3413
4.3393
4.3766
4.3459
4.3411
4.3433
4.3525
4.338.3
4.3954
BHV-6
Stop Start
Tare Nel Tlmo Time
4.2896 0.1052 13136.4 8007.0
4.3019 0.1551 8301 .6 8136.4
4.3425 0.0883 8468.4 8301 .6
4.3493 0.1287 8636.4 8468.4
4.2726 0.2274 8806.0 8636.4
4.2804 0.1007 8972.7 8806.0
4.3090 0.1638 9143.0 8972.7
4.3348 0.0797 9310.9 9143.0
4.3161 0.0861 9478.1 9310.9
4.3661 0.1054 9646.9 9478.1
4.3482 0.0656 9817.5 9646.9
4.3155 0.0782 9982.4 9817.5
4.3338 0.0547 10152.6 9982.4
4.31998 0.1107
Page2
Total Volume: 4.73E+06
Total Total Loading. Per Cent
Time Ute~$ mCI!m3 On Stream SCFM
7765.2 8,025,838 0.0131 77.0"k 36.5
9907.2 10,380,005 0.0149 114.7% 37.0
10012.8 10,490,644 0.0084 99.3".4 37.0
10078.8 10,559,794 0.0122 100.0% 37.0
10176.0 10,661 ,633 0.0213 101.0% 37.0
10000.8 10.478,072 0.0096 99.2% 37.0
10218.6 10,677,330 0.0153 101.4% 36.9
10073.4 10,525,612 0.0076 99.9% 36.9
10033.2 10,483,607 0.0082 99.5% 36.9
10125.0 10,493,516 0.0100 100.4% 36.6
10236.6 10,551,204 0.0062 101.6% 36.4
9&97.0 10,201,167 0.0077 98.2% 36.4
10212.6 10,526.466 0.0052 101.3% 36.4
f26737.2 134.054,886 0.0108 99.5% 36.8
Page 22 of 22
ATTACHMENTE
ENVIRONMENTAL GAMMA GRAPHS AND SUPPORTING DATA
I White Mesa Mill Ambient Gamma Levels Over Time-BHV-1 I
50.00~----------------------------------------------------------------------------------------------------------------------~
45.00 I
~oo I
~oo I
30.00
..... (])
t «l 25.00
:J ~ E
(]) a: 20.00
E
15.00
10.oo I
5.oo -1 • I a-H-li--1·1-++~
0·00 1~¥· itJi . -r .....-ei~~ ---=~·hiiiiiBIIfi ~ll¥ ..,._. ..... ........,.,. r ~ ~ -. 1111 :
9!3o;1981 9!3o;1983 9!3o;198s 913o;1987 913o;1989 9!3o;1991 9!3o;1993 9!3o;199s 913o;1997 9!3o;1999 9!3o;<oo1 9!3o;<oo3 913o;<oos 913o;<oo7 9!3o;<oo9 913o;<ot1 913of<ot3
Background (BHV-3) Subtracted from BHV-1
f ~~ I
I White Mesa MiiiAmbientGamma Levels Over Time BHV-21
50.00T-~--------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------~
45.00 +-----------------------------------------------------------------------------------------------------------------------------------------~
~00 I
35.00 +-----------------------------------------------------------------------------------------------------------------------------------------4
30.00 ,_
Q) t ~ ::J
J2" 25.00
E Q) a:
E 20.00
15.00 +---------------------------------------------------------------------------------------------------------------------------~
10.00 1-----------------~.-----------------------------------------------------------------------------------------------l
5.00 l'f II 11• e -... 'ff I
o.oo etP ,. .. ~ '~~ ·•··-• iii~ CP!Isdii · -,_.,...,... .. ~••v=JAIRIJ '~ .. .r:..nt . IIi •. ..,...-,,
3o-seP-8t 30-seP-89 30-Sep..gl 30-seP-05 30-seP-13
Background (BHV-3) Subtracted from BHV-2
I _.,_BHV-2 --]
I White Mesa Mill Ambient GammaL:eveiSOverTime-etiV-31
50.00
45.00
40.00
H
35.00 •
30.00
'-Q) t:: en .=l ~ 25.00
Q) a: E 20.00
I ... -~ j I .J. !
I ., 'N I l.. ,. ~ ~ J
-ft "-. ----fl------w--~-H-1 ,. ft II ~ r. ~ ~ ~ I' • w fl < ~ v
• j ~~ ~ n' vt ~~ ~ v ~·~ iA.J IJ 1l" ; • ... ~ ~ ~
' 'J ~· ' • ~ -w ,
15.00 w ~
I
10.00 --------------------~-----~------------ --·· ---- - -
5.00
0.00
3o-sep-B1 3CJ.seP-83 3CJ.seP-as 3CJ.seP-87 3CJ.seP-89 3CJ.seP-91 30..seP-93 3n~ 3n~ 3o..s 3n~ 3n~ 3n~ ~eP-9s ~eP-97 ep-99 ""<>eP-01 ""<>eP-03 ~eP-<Js 3n ~ 3o..s 30..S 3n ~ ~eP-<J7 ep-()9 eP-11 ~eP-13
c --------BHV-3 --,
[White-Mesa-Mill Ambient -Gamma Levels o-ver-Time -sH"v-41
50.00T---------------------------------------------------------------------------------------------------------------------~
~.oo +-----------------------------------------------------------------------------------------------------------------------4
40.00 +---------------------------------------------------------------------------------------------------------------------------------~
35.00 +-----------------------------------------------------------------------------------------------------------------------------4
30.00
'-Q) t 25.00 ro ::I .!:! E
Q) a: 20.00
E
15.00
10.00
5.00
000 ~ • -.. . . ... .-.-=..--.... .-.... ~ .,1 ••• ,
~-~ ~n -s ~-s -s ~-s ~-s ~-s ~ ~-~ ~ -s ~ ~ -s v-.,8P-81 -P-83 ~P-85 8P-87 8P-89 8P-91 8P-93 8P-9s 8P-97 -P-99 V-.;:)8P-01 8P-03 ""P-os 8P-07 8P-D9 veP-11 8P-13
Background (BHV-3) Subtracted from BHV-4
[--------BHV-4 I
I White Mesa Mill Ambient Gamma Levels Over Time--81-fV-5]
50.00~--------------------------------------------------------------------------------------------------------l
45.00 I
40.00 +-----------------------------------------------------------------------------------------------------1
35.00 r---------------------------------------_J
30.00 ,_
Q)
t ctS
::l
$! 25.00
E Q) a:
E 20.00
15.00 +---------------------------------------------------------------------------------------------------------4
10.00 +-------------------------------------------------------------~~----------------------------------------~
5.00 I ! I 1• -.... IWA 7'\:r..: l ..... nA I I .., -w I I 1: I I :.1:: II 'liP I -Ill ! \ _,
o.oo ••· --, =-, I ,.. • 1 • ·• 1e • ~e I 1• I 1 . • .... -1 ,
30-seP-81 30-Sep.&t 30-SeP-87 30-seP-9o 30-seP-93 30-Sep-96 30-seP-99 30-Sep.02 3o.seP-os 30-Sep.08 30-Sep-11
Background (BHV-3) Subtracted from BHV-5
I ~BHV-5 ~
1 White Mesa Mm Ambientciamma Le\.eJso~ernme 8Jiv-sl
50.00
45.00
40.00
35.00
30.00
..._
Q) t: ~ 25.00 -::::J
.!! E Q) a: 20.00 E
15.00
10.00 -
5.00
0.00 : _JiMM . .fY,. 4 --_.....,. --~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~~ ~ ~ft eP-81 eP-83 eP-85 ep..87 eP-89 ep..g1 ep..g3 ep..95 ep..97 ep..gg ep..ar »ep..a3 eP-as "eP-07 ---.:>ep..a9 »ep..11 ---.:>ep..13
Background (BHV-3) Subtracted from BHV-6
C ------~~BHV-6~-----I
Badge
Number
Control
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
45
46
47
51
52
53
64
White Mesa Mill Third Quarter 2013 Environmental Spherical Gamma Monitor Results
Location
Administration Vault
V205 Control Room
BHV-6
Ore Star.-Barrel Area
Vanadium Precip.Area
Y ellocake Drying Area
Leach
SAG Mill Control Room
Yellowcake Precip.
Central Control Room
Trammel Screen (ore pad)
North East Corner Ore Pad
Met. Lab
Filter Press Room
BHV-1
BHV-2
BHV-3
BHV-4
BHV-5
SAG Mill
Tails
CCD
North SX
Administration Building
Admin Parking Lot
Yellowcake Packaging
Yellowcake Storage
Bucking Room
Mill Lunch Room
South SX
Mtce. Super.'s Office
Ore Feed Grizzly
Scalehouse
Sample Plant (OBS)
Front Gate
AF -Barrel Dump Station
AF Circuit -South
AF Circuit-North
North Control # 1
North Control# 2
CaF2 Barrel Dump Station -
Operator Station
KF Barrel Dump Station
Date Issued
6126/2013
6/26/2013
612612013
612612013
612612013
612612013
612612013
612612013
612612013
6/2612013
6126/2013
6126/2013
612612013
6/26/2013
612612013
612612013
6126/2013
612612013
6/2612013
612612013
6126/2013
612612013
612612013
612612013
6126/2013
612612013
6126/2013
612612013
6/26/2013
6/2612013
612612013
612612013
612612013
612612013
6/26/2013
6/2612013
6/2612013
6/26/2013
6/2612013
612612013
612612013
612612013
Date
Returned
913012013
9130/2013
913012013
913012013
9130/2013
913012013
913012013
913012013
9130/2013
913012013
913012013
913012013
913012013
913012013
913012013
913012013
913012013
913012013
9130/2013
913012013
913012013
913012013
913012013
913012013
9130/2013
913012013
9130/2013
913012013
913012013
9130/2013
913012013
913012013
913012013
913012013
9130/2013
9130/2013
9130/2013
913012013
913012013
913012013
913012013
913012013
Total Days
Badge at
WMM
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
96
Ambient
Dose
Equivale
nt
34.6
50.5
30.4
305.8
71.8
302.7
138.6
406.8
295.5
91.9
139.8
360.2
66.4
173.2
33.5
31.5
29.6
34.5
34.6
466.8
58.6
80.3
59.5
40.4
90.5
1414
815.6
165.9
54.2
117.9
51.2
415.7
216.3
188.5
217.1
250.5
70.3
137.6
38.2
33.4
283
195.5
mRem I hour mRem I Day
0.02 0.360
0.02 0.526
0.01 0.317
0.13 3.185
0.03 0.748
0.13 3.153
0.06 1.444
0.18 4.238
0.13 3.078
0.04 0.957
0.06 1.456
0.16 3.752
0.03 0.692
0.08 1.804
0.01 0.349
0.01
0.01
0.01
0.02
0.20
0.03
0.03
0.03
0.02
0.04
0.61
0.35
0.07
0.02
0.05
0.02
0.18
0.09
0.08
0.09
0.11
0.03
0.06
0.02
0.01
0.12
0.08
0.328
0.308
0.359
0.360
4.863
0.610
0.836
0.620
0.421
0.943
14.729
8.496
1.728
0.565
1.228
0.533
4.330
2.253
1.964
2.261
2.609
0.732
1.433
0.398
0.348
2.948
2.036
mReml
Week
2.52
3.68
2.22
22.30
5.24
22.07
10.11
29.66
21.55
6.70
10.19
26.26
4.84
12.63
2.44
2.30
2.16
2.52
2.52
34.04
4.27
5.86
4.34
2.95
6.60
103.10
59.47
12.10
3.95
8.60
3.73
30.31
15.77
13.74
15.83
18.27
5.13
10.03
2.79
2.44
20.64
14.26
Badge
Number
Control
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
45
46
47
51
52
53
64
White Mesa Mill Fourth Quarter 2013 Environmental Spherical Gamma Monitor Results
Location
Administration Vault
V205 Control Room
BHV-6
Ore Star. -Barrel Area
Vanadium Precip.Area
Y ellocake Drying Area
Leach
SAG Mill Control Room
Yellowcake Precip.
Central Control Room
Trammel Screen (ore pad)
North East Corner Ore Pad
Met. Lab
Filter Press Room
BHV-1
BHV-2
BHV-3
BHV-4
BHV-5
SAG Mill
Tails
CCD
North SX
Administration Building
Admin Parking Lot
Yellowcake Packaging
Yellowcake Storage
Bucking Room
Mill Lunch Room
South SX
Mtce. Super.'s Office
Ore Feed Grizzly
Scalehouse
Sample Plant (OBS)
Front Gate
AF-Barrel Dump Station
AF Circuit-South
AF Circuit -North
North Control # 1
North Control # 2
CaF2 Barrel Dump Station -
Operator Station
KF Barrel Dump Station
Date Issued
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
9/30/2013
Date
Returned
112/2014
112/2014
112/2014
112/2014
1/2/2014
1/2/2014
112/2014
1/2/2014
1/2/2014
112/2014
112/2014
112/2014
1/2/2014
112/2014
1/2/2014
112/2014
112/2014
112/2014
112/2014
112/2014
1/2/2014
1/2/2014
112/2014
1/2/2014
112/2014
112/2014
112/2014
1/2/2014
112/2014
112/2014
1/2/2014
112/2014
1/2/2014
112/2014
1/2/2014
112/2014
1/2/2014
1/2/2014
1/2/2014
112/2014
1/2/2014
1/2/2014
Total
Days
Badge at
WMM
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
94
Mean
Ambient
Dose
Equivalent mRem I hour
36.2 0.02
49.3 0.02
33.7 0.01
659.6 0.29
128.5 0.06
145.7 0.06
176.7
377
160
82.6
142.4
337
84
186.4
38.9
33.3
31.4
32.1
38
381.1
62.6
84.5
99.5
44.2
85
1040
406
108.5
59.1
112.4
50.1
396.4
208
196.3
224.9
348.3
81.3
107.6
40.5
34.1
197
178.4
0.08
0.17
0.07
0.04
0.06
0.15
0.04
0.08
0.02
0.01
0.01
0.01
0.02
0.17
0.03
0.04
0.04
0.02
0.04
0.46
0.18
0.05
0.03
0.05
0.02
0.18
0.09
0.09
0.10
0.15
0.04
0.05
0.02
0.02
0.09
0.08
mRem/
Day
0.385
0.524
0.359
7.017
1.367
1.550
1.880
4.011
1.702
0.879
1.515
3.585
0.894
1.983
0.414
0.354
0.334
0.341
0.404
4.054
0.666
0.899
1.059
0.470
0.904
11.064
4.319
1.154
0.629
1.196
0.533
4.217
2.213
2.088
2.393
3.705
0.865
1.145
0.431
0.363
2.096
1.898
mRem/
Week
2.70
3.67
2.51
49.12
9.57
10.85
13.16
28.07
11.91
6.15
10.60
25.10
6.26
13.88
2.90
2.48
2.34
2.39
2.83
28.38
4.66
6.29
7.41
3.29
6.33
77.45
30.23
8.08
4.40
8.37
3.73
29.52
15.49
14.62
16.75
25.94
6.05
8.01
3.02
2.54
14.67
13.29
ATTACHMENT F
VEGETATION GRAPHS, DATA TABLE, LABORATORY RESULTS AND QNQC
(Log Scale)
__.
0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I I I
0 0 0 0 0 0 0
00 -....j 0) 01 ~ w 1\)
8/27/1981
8/27/1982
8/27/1983
8/27/1984
8/27/1985 -
8/27/1986
8/27/1987 -
8/27 I 1988 .,
8/27/1989 JJ D)
I
8/27/1990 1\)
1\)
0)
8/27/1991 -0 0
8/27/1992 -::::s n
(D
8/27/1993 -::::s ... ""' 8/27/1994 -D) ... c;·
f 8/27/1995 -::::s en
z 8/27/1996 -::::s m < 8/27/1997 -(D
Ul
T 8/27/1998 -(D ... D) ... z 8/27/1999 -c;· ::E ::::s
8/27/2000 -c t 8/27/2001 • 0
::::::.:
en 8/27/2002 " ::E Ul -8/27/2003
8/27/2004 -
8/27/2005 .
8/27/2006 -
8/27/2007 .
8/27/2008 -
8/27/2009 -
8/27/2010 -
8/27/2011 -
8/27/2012 -
8/27/2013 -
(Log Scale)
......
0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 00 -....! 0) c.n .j::>. VJ 1\)
8/27/1981
8/27/1982 -
8/27/1983
8/27/1984 -
8/27/1985
8/27/1986
8/27/1987
8/27/1988
"'tJ 8/27/1989 C" I
8/27/1990
1\) ......
0
8/27/1991 (')
0
8/27/1992 :::J
(')
CD
8/27/1993 :::J -""'' 8/27/1994 D) -a·
t 8/27/1995 :::J en
8/27/1996 --z :::J m < 8/27/1997 . CD
T
(Q
CD 8/27/1998 --D) -z 8/27/1999 a· ::E :::J
8/27/2000 -c t 8/27/2001 (')
:::::.:
(/) 8/27/2002 " ::E (Q -8/27/2003 "
8/27/2004
8/27/2005
8/27/2006
8/27/2007
8/27/2008
8/27/2009
8/27/2010 -
8/27/2011 -
8/27/2012
8/27/2013 .
WHITE MESA MILL
FORAGE RADIONUCLIDE DATA
NORTHEAST OF MILL
SAMPLED QTR. SAMPLED DATE
3rd'81 27-Aug-81
4th '81 20-0ct-81
2nd'82 15-Apr-82
3rd'82 01-Jul-82
4th '82 30-Nov-82
2nd '83 13-Apr-83
3rd '83 01-Jul-83
4th '83 30-Jan-84
2nd'84 28-Jun-84
4th '84 14-Nov-84
2nd'85 27-Mar-85
3rd '85 15-Jul-85
4th '85 09-0ct-85
2nd '86 24-Mar-86
3rd '86 lQ-Jul-86
4th '86 18-Dec-86
2nd'87 20-Apr-87
3rd'87 05-Jun-87
4th '87 22-Dec-87
2nd'88 19-Apr-88
3rd'88 28-Jul-88
2nd'89 07-Apr-89
3rd'89 06-Jun-89
4th '89 07-Nov-89
1st '90 17-Apr-90
2nd '90 20-Jun-90
3rd'90 17-0ct-90
1st '91 10-Apr-91
2nd'91 11-Jun-91
3rd'91 20-Nov-91
1st '92 22-Apr-92
2nd'92 10-Jun-92
3rd'92 10-Jun-92
1st '93 13-Apr-93
2nd '93 26-Jun-93
3rd '93 12-0ct-93
1st '94 11-May-94
2nd'94 19-Jul-94
3rd'94 28-Nov-94
1st '95 11-Apr-95
2nd'95 06-Jul-95
3rd '95 15-Nov-95
1st '96 23-Apr-96
2nd '96 * 31-Jul-96
3rd'96 14-Nov-96
1st '97 21-Apr-97
3rd'97 05-Sep-97
4th '97 20-Nov-97
1st '98 23-Mar-98
2nd'98 16-Jun-98
4th '98 05-Nov-98
2nd '99 15-Apr-99
3rd '99 07-Jul-99
4th '99 02-Dec-99
2nd'OO 21-Apr-00
2nd'OO 22-Jun-00
Ra-226
VALUE (uCi/Kg)
3.90E-04
1.40E-04
1.31E-04
1.60E-04
2.67E-06
9.36E-05
1.12E-04
1.09E-04
3.47E-04
5.61E-04
1.05E-03
8.20E-05
1.15E-04
5.72E-04
5.01E-04
8.70E-04
5.90E-04
1.60E-04
2.10E-04
4.50E-04
3.20E-05
5.60E-04
1.50E-04
6.00E-04
2.60E-04
1.80E-04
1.60E-04
1.20E-04
9.10E-05
4.50E-04
3.60E-05
1.00E-05
7.90E-05
3.70E-05
3.00E-05
6.60E-05
1.80E-04
1.71E-05
2.40E-04
6.70E-05
1.50E-05
5.50E-05
5.20E-05
3.00E-05
1.10E-05
l.lOE-05
8.00E-06
<9.10E-05
1.80E-05
5.70E-05
2.00E-04
6.03E-05
2.30E-05
1.50E-04
1.20E-06
Ra-226 LLD Pb-210 Pb-210 LLD
ERROR (uCI/Kg) uCi/Kg (S.OE-08) VALUE (uCI/Kg) ERROR (uCi/Kg) uCi/Kg (l.OE-06)
l.OOE-05 5.00E-08 l.lOE-03 1.00E-04 l.OOE-06
l.OOE-05 5.00E-08 6.80E-04 8.00E-05 l.OOE-06
1.30E-05 l.OOE-06 4.90E-04 7.00E-05 8.00E-05
1.00E-05 5.00E-08 8.00E-04 1.70E-04 1.00E-07
1.07E-06 1.00E-06 1.08E-04 9.00E-06 l.OOE-05
6.20E-06 8.00E-09 4.97E-04 9.30E-05 l.OOE-04
1.20E-05 6.00E-06 1.84E-04 1.20E-05 l.OOE-06
8.00E-06 4.00E-06 7.80E-04 6.20E-05 6.00E-05
1.20E-05 2.00E-09 3.75E-03 1.60E-04 4.00E-08
1.99E-04 2.00E-07 7.82E-03 3.30E-04 7.00E-08
3.00E-05 2.00E-06 3.22E-03 1.40E-04 2.00E-05
7.00E-06 3.00E-06 7.70E-04 1.30E-04 2.00E-04
l.OOE-05 3.00E-06 5.10E-04 3.00E-05 2.00E-05
2.10E-05 4.00E-06 2.49E-03 l.OOE-04 l.OOE-05
1.30E-05 3.00E-06 1.57E-03 1.70E-03 2.00E-04
5.00E-05 3.00E-06 6.80E-04 3.00E-05 3.00E-06
7.00E-05 5.00E-08 1.50E-03 1.00E-04 l.OOE-06
3.00E-05 5.00E-08 9.50E-04 4.00E-05 l.OOE-06
4.00E-05 5.00E-08 1.70E-03 l.OOE-04 l.OOE-06
7.00E-05 5.00E-08 1.40E-03 1.00E-04 1.00E-06
2.20E-05 5.00E-08 1.50E-04 4.40E-04 l.OOE-06
4.00E-05 *** 1.10E-03 l.OOE-01 ***
2.00E-05 *** 2.30E-04 2.00E-05 ***
5.00E-05 7.00E-06 2.04E-03 7.00E-05 1.40E-05
3.00E-05 4.00E-06 3.30E-04 2.00E-05 2.20E-05
2.00E-05 5.00E-08 3.20E-04 2.00E-05 l.OOE-06
2.00E-05 5.00E-08 3.30E-04 2.00E-05 l.OOE-06
2.00E-05 5.00E-06 3.00E-04 2.00E-05 1.00E-06
1.60E-05 2.00E-07 1.90E-04 2.00E-05 2.00E-07
4.00E-05 5.00E-08 1.09E-03 5.00E-05 l.OOE-06
1.00E-05 2.00E-06 1.50E-04 2.00E-05 l.OOE-05
7.00E-06 2.00E-07 7.50E-05 2.00E-05 l.OOE-06
3.50E-05 3.00E-06 7.10E-04 7.00E-05 2.00E-05
2.20E-05 3.00E-06 2.80E-04 3.00E-05 2.00E-05
1.50E-05 3.00E-06 4.30E-05 3.50E-05 2.00E-05
2.70E-05 3.00E-06 5.30E-04 6.00E-05 2.00E-05
4.00E-05 3.00E-05 4.40E-04 6.00E-05 2.00E-04
1.20E-06 9.00E-08 3.00E-05 6.10E-06 4.45E-06
1.50E-05 1.70E-07 1.70E-04 l.lOE-05 8.30E-07
5.40E-06 1.60E-07 1.40E-04 1.30E-05 7.90E-07
1.50E-06 1.50E-07 5.10E-05 4.50E-06 7.60E-07
5.00E-06 1.80E-07 6.70E-05 l.OOE-05 8.80E-07
2.50E-06 1.50E-07 3.20E-05 4.50E-06 1.80E-07
2.50E-06 1.80E-07 1.40E-04 7.10E-06 9.30E-07
4.70E-07 1.21E-07 4.10E-05 3.60E-06 6.10E-07
4.30E-07 1.33E-07 2.10E-05 7.30E-07 6.66E-07
1.20E-06 5.60E-07 1.40E-04 4.60E-06 l.lOE-07
9.10E-05 9.10E-05 <4.50E-04 4.50E-04 4.50E-04
1.20E-06 6.30E-08 4.00E-05 1.80E-06 3.20E-07
l.OOE-06 8.20E-08 8.70E-OS S.OOE-06 4.10E-07
3.00E-06 1.20E-07 3.00E-04 l .OOE-05 6.00E-05
1.40E-06 8.30E-08 1.40E-04 4.70E-06 4.20E-07
l.OOE-06 2.30E-07 2.10E-05 l.OOE-06 1.10E-06
3.00E-06 1.20E-07 1.60E-04 8.00E-06 5.90E-07
l.OOE-07 2.80E-07 1.60E-04 l.OOE-05 1.40E-06
4th '00 21-Dec-00 1.60E-06 l.lOE-06 3.70E-07 S.lOE-OS S.OOE-06 1.90E-06
1st '01 30-Apr-01 l.OOE-06 l.OOE-07 2.40E-07 <1.2E-06 l.OOE-07 2.40E-07
2nd'Ol 14-Jun-01 2.30E-06 2.00E-07 9.90E-08 3.80E-06 2.00E-07 S.OOE-07
4th '01 17-Dec-01 9.10E-06 2.40E-06 1.20E-07 3.57E-OS 2.97E-06 6.00E-07
1st '02 07-May-02 3.30E-OS 1.80E-06 7.60E-07 4.SOE-OS 2.61E-06 1.00E-OS
2nd'02 07-Jul-02 S.SSE-OS 2.81E-06 7.60E-07 S.31E-OS 3.90E-06 l.OOE-OS
4th '02 1S-Dec-02 7.7SE-OS 3.60E-06 7.60E-07 1.29E-04 6.15E-06 l.OOE-OS
1st '03 21-Mar-03 9.10E-06 1.30E-06 3.60E-07 1.13E-OS 1.61E-06 3.36E-06
2nd'03 10-Jun-03 2.SOE-OS 1.30E-06 3.60E-07 3.26E-06 2.00E-06 7.38E-08
4th '03 20-Nov-03 S.70E-OS 3.SOE-06 1.SOE-07 4.0SE-OS S.82E-06 8.30E-07
1st '04 08-Apr-04 9.38E-OS 3.70E-06 1.10E-07 S.88E-05 3.00E-06 S.SOE-07
2nd '04 12-Jun-04 S.63E-OS 3.40E-06 1.80E-07 6.42E-OS S.90E-06 9.00E-07
4th '04 30-Nov-04 8.41E-OS S.SOE-06 2.00E-08 2.48E-04 1.40E-05 3.00E-07
1st 'OS 21-Apr-OS S.60E-OS 3.00E-06 1.40E-07 S.80E-OS 4.00E-06 6.90E-07
2nd 'OS 13-Jun-OS 9.10E-06 l.SOE-06 1.80E-07 l.lOE-OS 1.20E-OS 9.00E-07
4th 'OS 10-Nov-OS 6.00E-OS 3.00E-06 l.lOE-10 1.70E-06 6.40E-07 S.SOE-10
1st '06 03-Apr-06 8.00E-OS S.OOE-06 S.OOE-08 3.40E-04 1.20E-OS l.OOE-06
2nd'06 16-Jun-06 4.10E-OS 3.10E-06 S.OOE-08 1.16E-04 6.10E-06 l.OOE-06
4th '06 28-Nov-06 1.17E-04 4.60E-06 1.90E-07 3.28E-04 9.SOE-06 9.SOE-07
1st '07 30-Mar-07 9.70E-OS 4.40E-06 1.90E-07 3.40E-04 8.70E-06 8.4-07
2nd'07 1-Jun-07 1.30E-OS 1.60E-06 1.90E-07 1.20E-04 6.60E-06 9.70E-07
4th '07 23-Nov-07 7.00E-OS 8.20E-06 2.00E-07 S.OOE-04 2.00E-OS 1.20E-06
1st '08 22-Apr-08 3.60E-06 3.00E-06 p.20E-07 2.30E-04 1.40E-OS l.OOE-06
2nd '08 18-Jun-08 3.20E-OS 3.20E-06 1.80E-06 6.90E-OS 3.50E-OS S.SOE-OS
4th '08 12-Dec-08 1.50E-04 S.20E-06 9.90E-07 3.60E-04 2.90E-OS 3.90E-OS
1st '09 28-Apr-09 5.90E-04 1.3SE-OS 1.SOE-06 3.40E-04 1.30E-OS 1.SOE-06
2nd '09 17-Jun-09 1.90E-OS 1.4SE-06 4.90E-07 3.60E-OS l.lOE-OS 1.80E-OS
4th '09 18-Dec-09 1.70E-04 S.90E-06 4.80E-04 1.20E-OS
1st '10 13-May-10 2.20E-04 7.20E-06 l.lOE-06 1.90E-04 1.90E-0S 2.90E-OS
2nd'10 18-Jun-10 G.SOE-OS 3.40E-06 7.60E-07 1.40E-04 1.90E-0S 2.90E-OS
4th '10 20-Dec-10 2.30E-OS 1.70E-06 S.20E-07 l.OOE-OS 1.SOE-06 2.30E-06
2nd '11 23-Jun-11 2.40E-07 1.40E-07 1.80E-07 <2.9E-06 1.70E-06 2.90E-06
3rd '11 27-Jul-11 4.90E-06 6.30E-07 3.20E-07 9.SOE-OS 2.10E-06 2.SOE-06
4th '11 23-Nov-11 7.20E-06 7.50E-07 2.90E-07 8.80E-08 4.30E-07 7.20E-07
2nd'12 11-Apr-12 4.40E-OS 1.90E-06 3.60E-07 2.10E-04 2.00E-06 1.00E-06
3rd '12 11-Jun-12 2.20E-OS 8.40E-07 l.lOE-07 1.30E-04 7.60E-06 S.90E-06
4th '12 06-Nov-12 3.10E-OS 4.82E-07 4.63E-08 4.26E-04 3.72E-06 6.S2E-07
2nd '13 30-Apr-13 1.14E-04 1.74E-06 S.34E-07 2.6SE-04 4.41E-06 S.37E-06
3rd '13 20-Jun-13 8.91E-OS 2.16E-06 1.42E-06 1.42E-04 3.68E-06 6.17E-06
4th '13 14-Nov-13 1.37E-04 3.87E-06 4.71E-06 S.33E-04 1.4SE-OS 2.27E-OS
*2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected dunng th1s penod
(Log Scale) .....
0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 co -...j (J) 01 .j:>. w ~
01-Jan-81
01-Jan-82 ::e
01-Jan-83 ::z: =t
01-Jan-84 m
3:
01-Jan-85 -m
(/)
01-Jan-86 · )>
3:
01-Jan-87 r= r-01-Jan-88 I
01-Jan-89 z 0
01-Jan-90 JJ -1 ::z:
01-Jan-91 m )>
01-Jan-92 (/) -1
01-Jan-93 · 0
t .,
01-Jan-94 3: -::D 01-Jan-95 " r-
~ -r-f,JJ N 01-Jan-96 0) -·S» -I
T
01-Jan-97 "N C.CN
-0)
"'0 01-Jan-98 S» 0" ::::s ~ 01-Jan-99 c.
0 "C 01-Jan-00 C" I N 01-Jan-01 ...a.
0
01-Jan-02 0 0
01-Jan-03 ::::s n CD 01-Jan-04 ::::s -..,
01-Jan-05 S» -01-Jan-06
c;·
::::s tn
01-Jan-07 ::::s
01-Jan-08 < CD
01-Jan-09 c.c !
01-Jan-10 S» -c;·
01-Jan-11 ::::s
01-Jan-12
01-Jan-13
01-Jan-14
WHITE MESA MILL
FORAGE RADIONUCLJDE DATA
NORTHWEST OF MILL
SAMPLED QTR. SAMPLED DATE
3rd '81 27-Aug-81
4th '81 20-0ct-81
2nd '82 15-Apr-82
3rd'82 01-Jul-82
4th '82 30-Nov-82
2nd'83 13-Apr-83
3rd'83 01-Jul-83
4th '83 30-Jan-84
2nd '84 28-Jun-84
4th '84 14-Nov-84
2nd '85 27-Mar-85
3rd '85 15-Jul-85
4th '85 09-0ct-85
2nd '86 24-Mar-86
3rd'86 10-Jul-86
4th '86 18-Dec-86
2nd'87 20-Apr-87
3rd'87 05-Jun-87
4th '87 22-Dec-87
2nd '88 19-Apr-88
3rd'88 28-Jul-88
2nd'89 07-Apr-89
3rd'89 06-Jun-89
4th '89 07-Nov-89
1st '90 17-Apr-90
2nd'90 20-Jun-90
3rd'90 17-0ct-90
1st '91 1Q-Apr-91
2nd '91 11-Jun-91
3rd'91 20-Nov-91
1st '92 22-Apr-92
2nd'92 10-Jun-92
3rd '92 10-Jun-92
1st '93 13-Apr-93
2nd'93 26-Jun-93
3rd'93 12-0ct-93
1st '94 11-May-94
2nd '94 19-Jul-94
3rd'94 28-Nov-94
1st '95 11-Apr-95
2nd '95 06-Jul-95
3rd '95 15-Nov-95
1st '96 23-Apr-96
2nd '96 * 31-Jul-96
3rd '96 14-Nov-96
1st '97 21-Apr-97
3rd'97 05-Sep-97
4th '97 2D-Nov-97
1st '98 23-Mar-98
2nd '98 16-Jun-98
4th '98 05-Nov-98
2nd '99 15-Apr-99
3rd '99 07-Jul-99
4th '99 02-Dec-99
2nd'OO 21-Apr-00
Ra-226
VALUE (uCi/Kg)
2.73E-03
2.00E-04
1.04E-04
2.00E-05
2.36E-06
8.58E-05
1.19E-04
9.78E-05
2.08E-04
6.05E-04
l.lOE-04
6.10E-05
1.07E-04
8.86E-04
6.66E-04
5.20E-04
4.10E-04
1.60E-04
3.60E-04
2.60E-04
3.10E-05
6.20E-04
3.40E-04
5.10E-04
3.60E-04
1.70E-04
8.80E-05
3.00E-04
3.10E-04
5.00E-04
2.00E-05
6.50E-06
1.20E-04
1.80E-05
5.20E-05
S.lOE-05
1.20E-04
3.73E-05
2.40E-04
8.40E-05
1.90E-05
1.20E-04
8.30E-05
3.60E-05
3.30E-05
5.40E·06
8.90E-06
<9.20E-05
< 6.SOE-08
4.20E-05
6.20E-05
5.45E-05
l.lOE-04
3.70E-05
Ra-226 LLD Pb-210 Pb-210 LLD
ERROR (uCi/Kg) uCI/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCI/Kg (1.0E-06)
5.00E-05 5.00E-08 7.10E-03 3.00E-04 l.OOE-06
l.OOE-05 5.00E-08 8.30E-04 5.00E-05 l.OOE-06
9.00E-06 7.00E-06 6.40E-04 5.00E-05 4.00E-05
l.OOE-05 5.00E-08 2.20E-04 9.00E-05 l.OOE-07
9.50E-07 l.OOE-06 8.00E-05 l.OOE-05 l.OOE-05
1.36E-05 2.00E-08 3.53E-04 1.90E-05 l.OOE-05
l.lOE-05 5.00E-06 1.58E-04 1.30E-05 1.00E-05
7.00E-06 2.00E-06 2.16E-03 3.40E-04 3.00E-04
l.OOE-05 3.00E-09 1.60E-03 7.00E-05 3.00E-08
1.64E-04 2.00E-07 2.58E-03 l.lOE-04 3.00E-08
8.00E-06 3.00E-06 8.63E-04 4.20E-05 3.00E-05
6.00E-06 2.00E-06 5.40E-04 5.00E-05 5.00E-05
6.00E-06 2.00E-06 3.80E-04 3.00E-05 2.00E-05
1.80E-05 2.00E-06 4.40E-03 1.90E-04 3.00E-05
1.80E-05 3.00E-06 4.78E-03 2.10E-04 6.00E-05
1.00E-04 3.00E-06 1.70E-03 1.00E-04 6.00E-05
l.OOE-04 5.00E-08 1.60E-03 1.00E-04 l.OOE-06
3.00E-05 S.OOE-08 5.50E-04 4.00E-05 l.OOE-06
5.00E-05 5.00E-08 1.80E-03 1.00E-04 l.OOE-06
5.00E-05 5.00E-08 1.90E-03 1.00E-04 l.OOE-06
1.90E-05 5.00E-08 1.60E-04 4.00E-05 l.OOE-06
5.00E-05 *** 1.70E-03 l.OOE-04 ***
3.00E-05 *** 7.40E-04 3.00E-05 ***
6.00E-05 7.00E-06 l.OOE-03 7.00E-05 1.40E-05
3.00E-05 4.00E-06 4.80E-04 2.00E-05 2.20E-05
2.00E-05 5.00E-08 3.20E-04 2.00E-05 l.OOE-06
1.60E-05 5.00E-08 2.90E-04 2.00E-05 l.OOE-06
3.00E-05 5.00E-06 4.10E-04 2.00E-05 1.00E-06
3.00E-05 2.00E-07 4.70E-04 2.00E-05 2.00E-07
4.00E-05 5.00E-08 l.SOE-03 l.OOE-04 1.00E-06
8.00E-06 2.00E-06 9.60E-05 1.40E-05 l.OOE-05
6.00E-06 2.00E-06 1.20E-04 2.00E-05 l.OOE-06
4.00E-05 3.00E-06 1.21E-03 8.00E-05 2.00E-05
1.70E-05 3.00E-06 2.10E-04 3.00E-05 2.00E-05
1.90E-05 3.00E-06 1.70E-05 3.60E-05 2.00E-05
2.30E-05 3.00E-06 7.10E-04 6.00E-05 2.00E-05
1.00E-05 3.00E-05 9.80E-04 1.60E-04 2.00E-04
1.60E-06 8.40E-08 7.80E-05 7.10E-06 4.20E-07
1.50E-05 1.70E-07 2.60E-04 1.30E-05 8.30E-07
6.10E-06 1.50E-07 1.20E-04 l.lOE-05 7.50E-05
1.50E-06 1.40E-07 4.SOE-05 4.30E-06 7.20E-07
6.80E-06 1.40E-07 l.OOE-05 5.80E-06 7.10E-07
3.30E-06 1.90E-07 6.80E-05 6.30E-06 1.80E-07
2.50E-06 1.60E-07 8.50E-05 5.60E-06 8.40E-07
2.30E-06 1.70E-07 4.40E-05 4.80E-06 8.40E-07
3.50E-07 1.56E-07 3.20E-05 9.00E-07 7.83E-07
7.20E-07 5.40E-07 3.40E-04 6.70E-06 l.lOE-07
9.20E-05 9.20E-05 <4.60E-04 4.60E-04 4.60E-04
6.50E-08 6.50E-08 <3.20E-07 3.20E-07 3.20E-07
l.OOE-06 l.lOE-07 1.70E-04 l.OOE-05 5.50E-07
l.OOE-06 l.OOE-07 1.40E-04 7.00E-06 l.OOE-07
1.40E-06 8.30E-08 9.20E-05 4.00E-06 4.20E-07
3.00E-06 2.20E-07 2.80E-05 l.OOE-06 l.lOE-06
1.00E-06 2.40E-07 2.70E-04 l.OOE-05 1.20E-06
2nd'OO 22-Jun-00 2.90E-05 l.OOE-06 3.30E-07 2.80E-04 2.00E-05 1.70E-06
4th '00 21-Dec-00 2.30E-06 1.40E-06 3.70E-07 3.30E-04 5.00E-05 1.90E-06
1st '01 30-Apr-01 2.10E-05 l.OOE-06 1.50E-07 <7.6E-07 N/A 7.60E-07
2nd'01 14-Jun-01 1.30E-06 4.00E-08 1.20E-07 1.80E-06 3.00E-08 5.90E-07
4th '01 17-Dec-01 3.70E-05 7.67E-07 8.30E-08 6.72E-05 2.62E-06 6.00E-07
1st '02 07-May-02 4.90E-05 2.40E-06 7.60E-07 1.28E-04 5.61E-06 l.OOE-05
2nd'02 07-Jul-02 8.88E-05 4.32E-06 7.60E-07 8.33E-05 4.32E-06 l.OOE-05
4th '02 15-Dec-02 1.50E-04 6.20E-06 7.60E-07 3.16E-04 1.07E-05 l.OOE-05
1st '03 21-Mar-03 5.00E-05 3.40E-06 2.71E-06 <4.2e-6 4.20E-06
2nd '03 10-Jun-03 5.60E-05 2.00E-06 4.10E-07 1.88E-04 5.14E-06 8.20E-08
4th '03 20-Nov-03 3.20E-04 8.20E-06 1.70E-07 4.89E-04 1.25E-05 8.30E-07
1st '04 08-Apr-04 6.29E-05 4.10E-06 2.00E-07 1.94E-05 4.00E-06 l.OOE-06
2nd'04 12-Jun-04 6.51E-05 3.40E-06 1.30E-07 1.87E-05 3.90E-06 6.50E-07
4th '04 30-Nov-04 7.50E-05 4.60E-06 2.00E-08 4.45E-04 1.40E-05 3.00E-07
1st '05 21-Apr-05 4.90E-05 2.70E-06 1.30E-07 1.27E-04 4.80E-06 6.50E-07
2nd'05 13-Jun-05 2.30E-05 2.10E-06 1.50E-07 4.70E-05 5.10E-06 7.60E-07
4th '05 10-Nov-05 7.40E-05 3.50E-06 1.20E-10 2.40E-06 8.10E-08 5.80E-10
1st '06 03-Apr-06 l.OOE-04 6.00E-06 5.00E-08 6.54E-04 1.50E-05 l.OOE-06
2nd'06 16-Jun-06 9.50E-05 5.90E-06 5.00E-08 4.48E-04 1.40E-05 l.OOE-06
4th '06 28-Nov-06 8.13E-05 4.10E-06 2.20E-07 3.25E-04 1.12E-06 l.OOE-05
1st '07 30-Mar-07 4.30E-05 2.60E-06 1.70E-07 2.64E-04 7.20E-06 8.60E-07
2nd '07 1-Jun-07 5.10E-05 3.20E-06 2.30E-07 5.30E-04 1.40E-06 1.20E-06
Mh '07 23-Nov-07 7.30E-05 6.60E-06 5.00E-08 7.00E-04 2.20E-05 1.10E-06
1st '08 22-Apr-08 2.80E-06 2.80E-06 7.20E-07 4.40E-04 2.00E-05 l.OOE-06
2nd'08 18-Jun-08 3.20E-06 3.30E-06 1.80E-06 1.40E-04 3.30E-05 5.50E-05
4th '08 12-Dec-08 7.30E-05 3.20E-06 7.40E-07 4.40E-04 2.50E-05 3.20E-05
1st '09 28-Apr-09 5.25E-05 3.60E-06 1.10E-06 1.90E-04 1.50E-05 2.20E-05
2nd '09 17-Jun-09 2.30E-05 1.60E-05 5.20E-07 4.30E-05 l.OOE-05 1.70E-05
4th '09 18-Dec-09 5.50E-05 3.50E-06 3.00E-04 l.lOE-05
1st '10 13-May-10 1.90E-04 6.10E-06 9.40E-07 5.10E-04 2.40E-05 3.10E-05
2nd'10 18-Jun-10 2.30E-05 2.00E-06 7.70E-07 8.30E-05 1.80E-05 2.90E-05
4th '10 20-Dec-10 8.60E-06 9.10E-07 3.90E-07 l.lOE-07 6.80E-07 l.lOE-06
2nd'11 23-Jun-11 2.10E-07 1.20E-07 1.40E-07 <2.2E-06 1.30E-06 2.20E-06
3rd '11 28-Jul-11 4.20E-06 5.40E-07 2.70E-07 2.30E-04 2.50E-06 2.30E-06
4th'11 23-Nov-11 7.70E-06 6.80E-07 2.30E-07 <5.8E-08 3.40E-07 5.80E-07
2nd '12 11-Apr-12 1.50E-05 9.50E-07 2.60E-07 <7.0E-07 6.00E-07 l.OOE-06
3rd '12 11-Jun-12 8.30E-06 5.40E-07 1.20E-07 1.40E-04 8.30E-06 6.50E-06
4th '12 06-Nov-12 2.34E-05 4.10E-07 7.71E-08 4.59E-04 3.83E-06 6.18E-07
2nd'13 30-Apr-13 9.04E-05 1.68E-06 8.58E-07 2.24E-04 4.46E-06 4.68E-06
3rd '13 20-Jun-13 2.58E-06 9.59E-07 8.06E-07 1.06E-04 2.30E-06 3.28E-06
4th '13 14-Nov-13 1.43E-04 3.70E-06 2.17E-06 4.65E-04 1.17E-05 1.80E-05
*2nd quarter of 1996 San Juan County, Utah, was declared a dtsaster area due to drought, no samples were collected dunng thts penod
(Log Scale)
...... ...... ......
0 0 0 0 0 0 0 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 CXl -....! en 01 .j:>. c.v I\)
I J :e 01-Jan-81
:I: =i 01-Jan-82
01-Jan-83 -m
:5:: m 01-Jan-84
(/)
)> 01-Jan-85 -
:5:: -01-Jan-86 r
01-Jan-87 · r
I
01-Jan-88 z 0 01-Jan-89 JJ .....
:I: :e m
01-Jan-90 ~
01-Jan-91 (/)
01-Jan-92 .....
0 "T1
5: -t 01-Jan-93 ~
01-Jan-94 ~
::D r '2' OJJ -·m -I ~N CCN
-0)
~ 01-Jan-95
1\)
(]) 01-Jan-96
T 01-Jan-97
m :::;, c.
"0
-o 01-Jan-98 0" ~ 01-Jan-99 0
C' I 01-Jan-00 N ......
0 01-Jan-01
0 0 01-Jan-02
::::J (') 01-Jan-03
CD :::;, -01-Jan-04 .., m -01-Jan-05 -
01-Jan-06
cs·
::::J th
01-Jan-07 -s·
< CD 01-Jan-08 ··
cc CD -01-Jan-09 ··
m -cs· 01-Jan-10 J
01-Jan-11 ::::J
01-Jan-12 -
01-Jan-13
01-Jan-14
WHITE MESA MILL
FORAGE RADIONUCLIDE DATA
SOUTHWEST OF MILL
SAMPLED QTR. SAMPLED DATE
3rd '81 27-Aug-81
4th '81 20-0ct-81
2nd'82 15-Apr-82
3rd '82 01-Jul-82
4th '82 30-Nov-82
2nd '83 13-Apr-83
3rd '83 01-Jul-83
4th '83 30-Jan-84
2nd '84 28-Jun-84
4th '84 14-Nov-84
2nd '85 27-Mar-85
3rd '85 15-Jul-85
4th '85 09-0ct-85
2nd'86 24-Mar-86
3rd'86 10-Jul-86
4th '86 18-Dec-86
2nd'87 20-Apr-87
3rd '87 05-Jun-87
4th '87 22-Dec-87
2nd '88 19-Apr-88
3rd '88 28-Jul-88
2nd'89 07-Apr-89
3rd'89 06-Jun-89
4th '89 07-Nov-89
1st '90 17-Apr-90
2nd '90 20-Jun-90
3rd'90 17-0ct-90
1st '91 10-Apr-91
2nd '91 11-Jun-91
3rd'91 20-Nov-91
1st '92 22-Apr-92
2nd'92 10-Jun-92
3rd'92 10-Jun-92
1st '93 13-Apr-93
2nd'93 26-Jun-93
3rd'93 12-0ct-93
1st '94 11-May-94
2nd'94 19-Jul-94
3rd'94 28-Nov-94
1st '95 11-Apr-95
2nd '95 06-Jul-95
3rd '95 15-Nov-95
1st '96 23-Apr-96
2nd '96 * 31-Jul-96
3rd'96 14-Nov-96
1st '97 21-Apr-97
3rd '97 05-Sep-97
4th '97 20-Nov-97
1st '98 23-Mar-98
2nd '98 16-Jun-98
4th '98 05-Nov-98
2nd'99 15-Apr-99
3rd'99 07-Jul-99
4th '99 02-Dec-99
2nd'OO 21-Apr-00
Ra-226 Ra-226
VALUE (uCi/Kg) ERROR (uCi/Kg)
9.50E-04 2.00E-05
3.00E-05 3.00E-06
1.37E-05 3.00E-06
3.40E-04 2.00E-05
1.75E-05 3.00E-06
7.13E-04 7.30E-05
5.39E-05 4.50E-06
6.40E-05 7.00E-06
8.27E-05 6.30E-06
2.72E-04 1.48E-04
4.73E-04 1.60E-07
6.60E-05 7.00E-06
2.83E-04 2.00E-05
1.57E-04 l.OOE-05
3.78E-04 1.00E-05
2.60E-04 2.00E-05
4.10E-04 7.00E-05
2.90E-04 4.00E-05
1.80E-04 3.00E-05
2.30E-04 5.00E-05
1.50E-04 3.00E-05
3.10E-04 4.00E-05
1.30E-04 2.00E-05
4.30E-04 5.00E-05
2.50E-04 3.00E-05
l.lOE-04 2.00E-05
6.10E-05 1.40E-05
3.40E-05 1.10E-05
8.00E-05 6.00E-06
6.50E-05 1.40E-05
l.GOE-05 7.00E-06
1.90E-05 l.OOE-05
l.GOE-05 1.80E-05
2.60E-05 2.00E-05
3.00E-05 1.40E-05
3.10E-05 l.GOE-05
2.00E-05 5.00E-06
1.75E-05 1.70E-06
l.OOE-04 9.00E-06
1.70E-05 1.50E-06
6.40E-06 6.00E-07
2.30E-05 2.20E-06
4.20E-05 2.20E-06
2.10E-05 2.00E-06
5.50E-06 4.20E-07
5.30E-06 3.20E-07
2.50E-05 9.50E-07
<7.90E-05 7.90E-05
3.60E-07 1.40E-07
4.30E-05 l.OOE-06
2.40E-05 l.OOE-06
2.23E-05 8.60E-07
1.50E-04 3.00E-06
l .OOE-04 2.00E-06
LLD Pb-210 Pb-210 LLD
uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (1.0E-06)
5.00E-08 1.50E-04 l.OOE-05 l.OOE-06
5.00E-08 1.50E-04 2.00E-05 1.00E-06
3.00E-06 3.80E-04 4.00E-05 4.00E-05
5.00E-08 3.68E-03 2.70E-04 1.00E-07
2.00E-06 7.92E-04 4.00E-06 2.00E-05
9.00E-08 2.51E-03 3.00E-04 3.00E-04
2.00E-06 6.88E-04 4.30E-05 4.00E-05
4.00E-06 1.20E-03 l.OOE-04 4.00E-05
3.00E-09 1.80E-03 l.OOE-04 9.00E-08
2.00E-07 4.70E-03 7.20E-04 3.00E-07
3.00E-06 7.07E-04 3.60E-05 3.00E-05
4.00E-06 4.90E-04 3.00E-05 3.00E-05
7.00E-06 1.50E-03 l.OOE-04 7.00E-05
4.00E-06 4.14E-03 1.80E-04 3.00E-05
2.00E-06 1.65E-02 7.00E-04 1.00E-04
2.00E-06 1.70E-03 l.OOE-04 1.00E-04
5.00E-08 2.20E-03 l.OOE-04 l.OOE-06
5.00E-08 7.50E-04 5.00E-05 l.OOE-06
5.00E-08 2.40E-03 l .OOE-04 l.OOE-06
5.00E-08 2.90E-03 l.OOE-04 l.OOE-06
5.00E-08 4.30E-03 2.00E-04 l.OOE-06
*** 4.20E-03 l.OOE-04 ***
*** 1.50E-03 l.OOE-04 ***
1.40E-05 3.50E-03 1.40E-04 2.70E-05
5.00E-06 2.39E-03 5.00E-05 2.50E-05
5.00E-08 6.60E-04 3.00E-05 1.00E-06
5.00E-08 6.10E-04 3.00E-05 l.OOE-06
5.00E-06 2.20E-04 l.OOE-05 l .OOE-06
2.00E-07 1.20E-04 l.OOE-05 2.00E-07
5.00E-08 9.10E-04 5.00E-05 l.OOE-06
2.00E-06 3.20E-04 2.00E-05 l.OOE-05
2.00E-07 2.20E-04 2.00E-05 l.OOE-06
3.00E-06 7.60E-04 6.00E-05 2.00E-05
3.00E-06 3.40E-04 3.00E-05 2.00E-05
3.00E-06 O.OOE+OO 3.00E-05 2.00E-05
3.00E-06 4.20E-04 6.00E-05 2.00E-05
3.00E-05 3.90E-04 8.00E-05 2.00E-04
7.60E-08 1.30E-04 7.80E-06 3.80E-07
1.50E-07 2.60E-04 1.20E-05 7.40E-07
1.60E-07 1.60E-04 1.50E-05 8.10E-07
1.40E-07 4.40E-05 4.20E-06 7.00E-07
1.70E-07 6.60E-05 9.60E-06 8.30E-07
1.70E-07 1.00E-04 6.70E-06 1.80E-07
1.60E-07 1.90E-04 7.30E-06 8.20E-07
1.40E-07 3.30E-05 3.90E-06 7.00E-07
1.26E-07 1.90E-05 6.90E-07 6.34E-07
5.90E-07 1.30E-04 4.70E-06 1.20E-07
7.90E-05 <3.90E-04 3.90E-04 3.90E-04
3.30E-08 <1.7E-07 1.70E-07 1.70E-07
7.60E-08 2.50E-04 l.OOE-05 3.80E-07
1.20E-07 1.70E-04 8.00E-06 6.20E-07
1.20E-07 2.30E-04 7.00E-06 5.90E-07
2.00E-07 1.70E-05 l.OOE-06 l.OOE-06
1.20E-07 l .lOE-04 7.00E-06 6.10E-07
2nd'OO 22-Jun-00 1.30E-06 l.OOE-07 2.40E-07 2.00E-04 l .OOE-05 1.20E-06
4th '00 21-Dec-00 1.20E-06 9.00E-07 2.40E-07 1.20E-04 3.00E-05 1.20E-06
1st '01 30-Apr-01 1.80E-06 l .OOE-07 1.70E-07 <8.3E-07 N/A 8.30E-07
2nd '01 14-Jun-01 2.60E-06 2.00E-07 9.90E-08 l.lOE-06 2.00E-08 5.00E-07
4th '01 17-Dec-01 2.63E-06 4.60E-05 1.20E-07 9.40E-05 3.72E-06 6.00E-07
1st '02 07-May-02 3.50E-05 2.20E-06 7.60E-07 1.36E-04 5.61E-06 l.OOE-05
2nd'02 07-Jul-02 4.02E-05 2.34E-06 7.60E-07 7.04E-05 4.11E-06 l.OOE-05
4th '02 15-Dec-02 8.10E-05 3.90E-06 7.60E-07 2.87E-04 8.54E-06 l.OOE-05
1st '03 21-Mar-03 3.70E-05 2.60E-06 2.41E-06 2.69E-05 2.01E-06 3.73E-06
2nd'03 10-Jun-03 1.30E-05 1.00E-06 5.20E-07 <l.OOE-07 l.OOE-07
4th '03 20-Nov-03 1.60E-04 1.30E-05 1.20E-07 1.42E-04 6.42E-06 5.90E-07
1st '04 08-Apr-04 1.40E-04 7.70E-06 l.lOE-07 6.10E-06 2.70E-06 5.50E-07
2nd '04 12-Jun-04 6.51E-05 3.20E-06 1.50E-07 5.27E-05 4.90E-06 7.60E-07
4th '04 30-Nov-04 8.40E-05 5.70E-06 3.00E-08 3.39E-04 l.GOE-05 3.00E-07
1st '05 21-Apr-05 1.70E-05 1.60E-06 1.30E-07 4.50E-05 3.50E-06 6.50E-07
2nd '05 13-Jun-05 1.50E-05 1.60E-06 1.40E-07 7.00E-05 5.10E-06 6.90E-07
4th '05 10-Nov-05 3.80E-05 2.10E-06 8.60E-10 1.20E-06 4.80E-08 4.30E-10
1st '06 03-Apr-06 l.OOE-04 6.00E-06 5.00E-08 3.30E-04 1.10E-05 l.OOE-06
2nd'06 16-Jun-06 3.40E-05 2.50E-06 5.00E-08 1.37E-04 6.00E-06 l.OOE-06
4th '06 28-Nov-06 7.31E-05 3.20E-06 1.60E-07 2.98E-04 8.50E-06 8.20E-07
1st '07 30-Mar-07 3.00E-05 2.20E-06 1.70E-07 3.20E-04 7.90E-06 8.40E-07
2nd'07 1-Jun-07 1.10E-04 4.60E-06 2.3-07 3.20E-04 1.10E-05 1.10E-06
4th '07 23-Nov-07 5.60E-05 5.20E-06 5.00E-08 6.40E-04 1.90E-05 1.00E-06
1st '08 22-Apr-08 3.20E-05 2.30E-06 7.20E-07 2.30E-04 1.50E-05 l.OOE-06
2nd'08 18-Jun-08 1.25E-05 2.20E-06 1.80E-06 5.00E-05 3.00E-05 4.80E-03
4th '08 12-Dec-08 9.20E-05 4.10E-06 9.60E-07 4.10E-04 3.00E-05 4.00E-05
1st '09 28-Apr-09 2.60E-05 2.90E-06 1.40E-06 3.70E-05 1.50E-06 2.50E-05
2nd '09 17-Jun-09 2.40E-05 1.40E-06 3.90E-07 3.50E-05 7.90E-06 1.30E-05
4th '09 18-Dec-09 3.10E-05 2.30E-06 2.10E-04 8.40E-06
1st '10 13-May-10 2.00E-05 2.10E-06 '9.40E-07 5.60E-05 1.50E-05 2.40E-05
2nd'10 18-Jun-10 l.lOE-05 1.30E-06 6.60E-07 7.80E-05 1.60E-05 2.50E-05
4th '10 20-Dec-10 6.70E-06 9.10E-07 4.80E-07 8.00E-07 7.90E-07 1.30E-06
2nd '11 23-Jun-11 <1.7E-07 6.90E-08 1.70E-07 <2.5E-06 1.50E-06 2.50E-06
3rd '11 27-Jul-11 1.60E-05 l.OOE-06 2.60E-07 9.50E-05 1.60E-06 1.70E-06
4th '11 23-Nov-11 7.80E-07 2.50E-07 2.30E-07 <5.9E-07 3.50E-07 5.90E-07
2nd '12 11-Apr-12 5.00E-06 6.00E-07 3.00E-07 <7.0E-07 7.00E-07 1.00E-06
3rd '12 11-Jun-12 1.90E-08 6.20E-08 l.lOE-07 <2.5E-07 1.30E-06 2.20E-06
4th '12 06-Nov-12 1.49E-05 3.41E-07 4.25E-08 4.45E-04 4.01E-06 8.57E-07
2nd '13 30-Apr-13 4.50E-05 1.19E-06 5.39E-07 3.62E-04 6.30E-06 9.90E-06
3rd '13 20-Jun-13 1.51E-05 1.06E-06 1.96E-06 6.71E-05 2.93E-06 6.24E-06
4th '13 14-Nov-13 1.18E-04 3.39E-06 2.97E-06 5.92E-04 1.27E-05 1.62E-05
*2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period
(Log Scale)
...... ...... ...... ...... ...... ...... ...... ......
0 0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0
m m m m m m m m m
I I I I I I I I + 0 0 0 0 0 0 0 0 0
CXl ""~ O'l 01 ~ w 1\:) ...... 0
01-Jan-81
== 01-Jan-82 %
::::j
01-Jan-83 m
01-Jan-84 s: m
01-Jan-85
(/)
)>
01-Jan-86 == F
01-Jan-87 r-
I
01-Jan-88 (/)
0
01-Jan-89 c -t
01-Jan-90 :I:
== 01-Jan-91 m (/)
01-Jan-92 -t
0 01-Jan-93 t "'T1
01-Jan-94 == -:IJ r-
:t', 01-Jan-95 '2'
1\J OJJ CD 01-Jan-96 -·m -I
f ""' 01-Jan-97 CCN
-0) -a 01-Jan-98 m 0" "' :::J
~ 01-Jan-99 a.
0 "'tJ
01-Jan-00 tT I N ......
01-Jan-01 0
01-Jan-02 0 0 :::J 01-Jan-03 ()
CD
01-Jan-04 :::J -""' 01-Jan-05 -m -s·
01-Jan-06 -:::J tn
01-Jan-07 s·
01-Jan-08 < CD co
01-Jan-09 CD -m
01-Jan-10 -s·
01-Jan-11 :::J
01-Jan-12
01-Jan-13 .,
01-Jan-14 ·1
m¥11 [ Laboratories LLC
a member of The GEL Group INC PO Bo~ 30712 Charleston, SC 29417
2040 Savage Road Charleston, SC 29407
P 843.556.8171 F 843.766.1178
December 16,2013
Ms. Kathy Weinel
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Re: Vegetation Analysis
Work Order: 337777
Dear Ms. Weinel:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on November 19, 2013. This original data report has been prepared and reviewed in
accordance with GEL's standard operating procedures.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 4505.
Purchase Order: DW16138
Enclosures
Sincerely
Heather Shaffer
Project Manager
II 1111111111111111111111
www.get.com
Energy Fuels Resources (USA), Inc.
Vegetation Analysis
SDG: 337777
Case Narrative
Page 1 of20
Page 2 of20
December 16,2013
Laboratory Identification:
GEL Laboratories LLC
2040 Savage Road
Charleston, South Carolina 29407
[phone]
Summary:
Receipt Narrative
for
Energy Fuels Resources (USA), Inc.
SDG: 337777
Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on November 19,
2013 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All
sample containers arrived without any visible signs of tampering or breakage. There are no additional comments
concerning sample receipt.
Sample Identification: The laboratory received the following samples:
Laboratory ID Client ID
337777001 North East
337777002 North West
337777003 South East
Case Narrative:
Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any
technical or administrative problems during analysis, data review, and reduction are contained in the analytical
case narratives in the enclosed data package.
The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt
Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry.
Heather Shaffer
Project Manager
Page 3 of20
Chain of Custody and
Supporting
Documentation
337777
Sheet 1 of 1
CHAIN OF CUSTODY
Samples Shipped to: Gel Laboratories Contact: Garrin Palmer ~2~0~40~S~a~v~ag~e~R~oa-d~------------Ph:4356784115
Charleston, SC 29407 [e-mail]
Chain of Custody/Sampling Analysis Request
p . ro)ec1 s amp1ers N a me s amp1ers tgnature
. ~~~ .....__
Late Fall Vegetation 2013 Garrin Palmer L ~.:> .. ~
Time
Sample ID Date Collected Collected Laboratory Analysis Requested
North East 11/14/2013 1200 Ra 226, PB-21 0
North West 11/14/2013 1245 Ra 226, PB-21 0
South East 11/14/2013 1345 Ra 226, PB-21 0
Comments:
Relinq.uished By:(Sig~r~ Date/Time Received By:(Signature) Date/Time
6~ 1-r::.-11/1 '1{ 1.3 fete ChA~. 11-l~-1~
~-oCJ
Relinquished By:(Signature) Date/Time ReceljtectJly:(Signature) Date/Time
m:3! j Laboratories tJc SAMPLE RECEIPT & REVIEW FORM
Clit!nt: ~ )tJ Vi\\ SDG/ARJCOC/Work Order: .1 "">11] l
Rc.:clvcd U}': <) v? Dutn Received: )\-JCJ--11
Suspected Hazard Information ~ Q +If Net Counts> IOOcpm on samples not marked "radioactive", contact the Radiation Safety Group for further z investigation.
.COC/Samples marked as radioactive? / [IV!aximum Net Counts Observed* (Observed Counts-Area Background Counts): ("J c 11\ 111/\
Classified Radioactive II or Ill by RSO? ~f yes, Were swipes taken of sample contatiners < action levels? T
COC/Samples marked containing PCBs? ~
Package, COC, and/or Samples marked as {/
beryllium or asbestos containing? 1/ l)f_yes, samples arc to be segregeated as Safety Controlled Samples, and opened by the GEL Safety Group.
Shipped as a DOT Hazardous? / IJ-Iazard Class Shipped: UN#:
Samples identified as Foreign Soil? /
Sample Receipt Criteria ~ ~ :l ~ ·~ rs (R~ed for Non-Co ·•· , """!;_ Item'i) "'
!Shipping containers received intact v~ Circle Applicable:
1 I and sealed? Seals broken Damaged container Leaking cont~ther (describe)
Samples requiring cold preservation Presenoation Method: Ice bugs Blue ice Drydi~;~ Other (describe) 2 within (0 < 6 deg. C)?* v jt{ •all tempemtures are recorded in
2a Daily check performed and passed on '""'l"''"'uoo Device Serial#: : ~~!?#~fYp$c~le~ (
IR temperature gun? §I .. , Tempemture Device
3 Chain of custody documents included
with shipment?
Circle Applicable:
4 !Sample containers intact and sealed? Seals broken Damaged container Leaking container Other (describe)
I
Lc;:omniP< requiring chemical Sample ID's, containers affected and obsenoed pH:
5 I preservation at proper pH? v llf t added. Lot#:
VOA vials free of heads pace (defined v !Sample ID's and containers affected:
6 as< 6mm bubble)?
7 Are Encore containers present?
"yes, immediately deliver to Volatiles labomtory)
Samples received within holding liD's and tests affected:
8 time?
Sample !D's on COC match !D's on ; !Sample ID's and containers affected:
9 I bottles?
!Date & time on COC match date & !Sample ID's affected:
10 time on bollles?
JNumoer of conlainers received match !Sample !D's affected:
11 I number indicated on COC? 0\'\.t Y76t ID
12 Are sample containers identifiable as ~
GEL provided?
13 COC form is properly signed in
relinquished/received sections?
Fed Ex Air Fed Ex Ground Field Services ®licable:
Courier Other
lZ > 81 ~y~ oz qu?q 8Y7CJ
14 Carrier and tracking number. ,, I . I' I I q_u1'8 U.257 ,, I , I \ 'I. 9 57 I ~LDO\
(Use Ctintinunrlon Form if needed):
PM (or PMA) review: Initials Date _ LL__..Ig _/3 _ Page_1of -f--
GEL Laboratories LLC -Login Review Report Report Date: 16-DEC-13
Work Order: 337777
Page 1 of 2
GEL Work Order/SDG: 337777
Client SDG: 337777
Late Fall Vegetation 2013 Work Order Due Date: 19-DEC-13
Package Due Date: 16-DEC-13
Collector: C
Prelogin #: 20131110591
Project Workdef ID: 1310529
SDG Status: Closed
Logged by:
Project Manager:
Project Name:
Purchase Order:
Package Level:
EDD Format:
Heather Shaffer
DNMI00101 Vegetation Analysis
DW16138
LEVEL3
EIM_DNMI
GELID Client Sample ID Client Sample Desc.
337777001 North East
337777002 North West
337777003 South East
Client Sample ID
-001 North East
-002 North West
-003 South East
Status Tests/Methods
REVW GFPC, Total Alpha Radium, solid
REVW GFPC, Pb210, Solid
REVW Laboratory Composite -Dry prep
instructions
REVW GFPC, Total Alpha Radium, solid
REVW GFPC, Pb210, Solid
REVW Laboratory Composite -Dry prep
instructions
REVW GFPC, Total Alpha Radium, solid
REVW GFPC, Pb210, Solid
REVW Laboratory Composite -Dry prep
instructions
Collect
Date & Time
EDD Due Date:
Due Date:
HXS1
Receive Time # of
Date & Time Zone Cont.
14-NOV-13 12:00 19-NOV-13 09:00 -2
14-NOV-13 12:45 19-NOV-13 09:00 -2
14-NOV-13 13:45 19-NOV-13 09:00 -2
Product
Reference Fax Date PM Comments
Product: LABCOMP_S WorkdefiD: 1310628
Method:
In Product Group? No Group Name:
Product Description: Laboratory Composite-Dry prep instructions
Samples: 001, 002, 003
Parmname Check: All parmnames scheduled properly
CAS# Parmname
Client RDL or
PQL & Unit
18-DEC-13
19-DEC-13
Lab
Matrix
Fax Days to
Due Date Process
VEGETATION
VEGETATION
VEGETATION
30
30
30
Aux Data
Client Matrix SOLID
Cooler Seal Undisturbed y
Temperature (C) 19
Client Matrix SOLID
Cooler Seal Undisturbed y
Temperature (C) 19
Client Matrix SOLID
Cooler Seal Undisturbed y
Temperature (C) 19
Group Reference:
CofC#
Path: Rad Prep SPRP
Product Reference:
Prelog Lab Field
Group QC QC
Receive
Codes
Moisture Correction: "As Received"
Reporting
Units
Parm Included Included Custom
Function in Sample? in QC? List?
No
0 N c....,
0
\0
(!,) on C';$
0-.
GEL Laboratories LLC -Login Review Report
Product: GFC_PBS WorkdefiD: 1310600 In Product Group? No
Method: DOE RP280 Modified
Product Description: GFPC, Pb210, Solid
Samples: 001, 002, 003
Parmname Check: All parmnames scheduled properly
CAS# Parmname
14255-04-0 Lead-210
Product: GFCTORAS WorkdefiD: 1310679 In Product Group? No
Method: EPA 900.1 Modified
Product Description: GFPC, Total Alpha Radium, solid
Samples: 001, 002, 003
Parmname Check: All parmnames scheduled properly
CAS# Parmname
Total Radium
Action Product Name Description
Contingent
Tests
Login Requirements:
Requirement
Are these vegetation sample?
Login Reminder?
Group Name:
Client RDL or
PQL & Unit
.000001
Group Name:
Client RDL or
PQL & Unit
.00000005
Samples
Reporting
Units
uCi/kg
Reporting
Units
uCi/kg
Include? Comments
Group Reference:
Report Date: 16-DEC-13
Work Order: 337777
Page 2 of 2
Path: Standard
Product Reference:
Moisture Correction: "As Received"
Parm Included Included Custom
Function in Sample? in QC? List?
REG y y
Group Reference:
Path: Standard
Product Reference:
Yes
Moisture Correction: "As Received"
Parm Included Included Custom
Function in Sample? in QC? List?
REG y y Yes
y
y
FOR VEGETATION: After logging in, change from DRY to WET in sample inquiry.
FOR VEGETATION: After logging in, change from DRY to WET in sample inquiry. Log
with lab camp.
Peer Review by: ___________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? _____ _
0 N
'"'"""' 0
r-
(1)
b1)
ell p..
Page 8 of20
Laboratory
Certifications
List of current GEL Certifications as of 16 December 2013
State Certification
Alaska UST-110
Arkansas 88-0651
CLIA 42D0904046
California NELAP 01151CA
Colorado SC00012
Connecticut PH-0169
Delaware SC000122013-10
DoD ELAP/ ISO 17025 A2LA 2567.01
Florida NELAP E87156
Foreign Soils Permit P330-12-00283,P330-12-00284
Georgia SC00012
Georgia SDWA 967
Hawaii SCOOOI22013-IO ----Idaho Chemistry SC00012
Idaho Radiochemistry SC00012
Illinois NELAP 200029
Indiana C-SC-01
Kansas NELAP E-10332
Kentucky 90129
Louisiana NELAP 03046 (AI33904)
Louisiana SDW A LA130005
Maryland 270
Massachusetts M-SC012
Michigan 9976
Mississippi SC000122013-10
Nebraska NE-OS-26-13
Nevada SC000122014-1
New Hampshire NELAP l 2054
New Jersey NELAP I SC002
New Mexico SC00012
New York NELAP 11501
North Carolina 233
North Carolina SDWA 45709
Oklahoma 9904
Pennsylvania NELAP 68-00485
Plant Material Permit PDEP-12-00260
South Carolina Chemistry 10120001
South Carolina GVL 23611001
South Carolina Radiochemi 10120002
Tennessee TN 02934
TexasNELAP T104704235-13-8
UtahNELAP SC000122013-11
Vermont VT87156 -Virginia NELAP 460202
Washington C780-12
Wisconsin 999887790
Page 9 of20
Page 10 of20
Method/Analysis Information
Radiochemistry Case Narrative
Energy Fuels Resources (DNMI)
SDG 337777
Product: GFPC, Pb210, Solid
Analytical Method: DOE RP280 Modified
Prep Method: Dry Soil Prep
Analytical Batch Number: 1348205
Prep Batch Number: 1348020
Sample ID
337777001
337777002
337777003
1202990210
1202990211
1202990212
1202990213
Client ID
North East
North West
South East
Method Blank (MB)
337777001(North East) Sample Duplicate (DUP)
33777700l(North East) Matrix Spike (MS)
Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
SOP Reference
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with
GL-RAD-A-018 REV# 13.
Calibration Information:
Calibration Information
All initial and continuing calibration requirements have been met.
Standards Information
Standard solutions for these analysis are NlST traceable or verified with a NlST traceable standard and used
before the expiration dates.
Sample Geometry
All counting sources were prepared in the same geometry as the calibration standards.
Ouality Control (OC) Information:
Blank Information
The blank volume is representative of the sample volume in this batch.
Page 11 of20
Designated QC
The following sample was used for QC: 337777001 (North East).
QC Information
All of the QC samples meet the required acceptance limits with the following exceptions: The blank,
1202990210 (MB), did not meet the detection limit due to keeping the blank volume consistent with the other
sample aliquots. All other samples met the detection limits. The blank 1202990210 (MB) result is greater than
the required detection limit but less than the MDC.
Technical Information:
Holding Time
All sample procedures for this sample set were performed within the required holding time.
Sample Re-prep/Re-analysis
Samples 1202990210 (MB), 1202990211 (North East), 337777001 (North East), 337777002 (North West) and
337777003 (South East) were recounted to confirm sample results. The original counts are reported.
Chemical Recoveries
All chemical recoveries meet the required acceptance limits for this sample set.
Miscellaneous Information:
Data Exception (DER) Documentation
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
SOP or contractual documents. A data exception report (DER) was not generated for this SDG.
Additional Comments
Additional comments were not required for this sample set.
Qualifier Information
Manual qualifiers were not required.
Method/ Analysis Information
Product: GFPC, Total Alpha Radium, solid
Analytical Method: EPA 900.1 Modified
Prep Method: Dry Soil Prep
Analytical Batch Number: 1348207
Prep Batch Number: 1348020
Sample ID
337777001
337777002
337777003
1202990217
Client ID
North East
North West
South East
Method Blank (MB)
Page 12 of20
1202990218
1202990219
1202990220
337777001(North East) Sample Duplicate (DUP)
337777001(North East) Matrix Spike (MS)
Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
SOP Reference
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with
GL-RAD-A-010 REV# 15.
Calibration Information:
Calibration Information
All initial and continuing calibration requirements have been met.
Standards Information
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
before the expiration dates.
Sample Geometry
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control (OC) Information:
Blank Information
The blank volume is representative of the sample volume in this batch.
Designated QC
The following sample was used for QC: 337777001 (North East).
QC Information
All of the QC samples meet the required acceptance limits with the following exceptions: Refer to Data
Exception Report (DER). The blank, 1202990217 (MB), did not meet the detection limit due to keeping the
blank volume consistent with the other sample aliquots. All other samples met the detection limits.
Technical Information:
Holding Time
All sample procedures for this sample set were performed within the required holding time.
Sample Re-prep/Re-analysis
None of the samples in this sample set required reprep or reanalysis.
Chemical Recoveries
All chemical recoveries meet the required acceptance limits for this sample set.
Miscellaneous Information:
Data Exception (DER) Documentation
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
SOP or contractual documents. The following DER was generated for this SDG: DER 1252304 was generated
due to Failed Recovery for MS/PS. 1. The matrix spike 1202990219 does not meet the recovery requirement due
to the matrix of the sample. 1. Reporting results.
Page 13 of20
Additional Comments
Additional comments were not required for this sample set.
Qualifier Information
Manual qualifiers were not required.
Certification Statement
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 14 of20
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone]-www.gel.com
Qualifier Definition Report
for
DNMIOOI Energy Fuels Resources (USA), Inc.
Client SDG: 337777 GEL Work Order: 337777
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a surrogate compound
U Analyte was analyzed for, but not detected above the CRDL.
ReviewN alidation
GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables
receive a third level review of the fractional data package.
The following data validator verified the information presented in this data report:
Signature: 9l 0 G..JJ.-u <J · IY.. <.__ ( lt! (i' tj
Date: 19 DEC 2013
Name: Heather McCarty
Title: Analyst II
GEL Laboratories LLC
Fonn GEL-DER
DATA EXCEPTION REPORT
Mo.Day Yr.
17-DEC-13
Division:
Radiochemistry Specifications ---l Quality Criteria:
Instrument Type: Test I Method: Matrix Type:
GFPC EPA 900.1 Modified Solid ------------------------------------------------------------
Batch ID:
1348207
Sample Numbers:
See Below
Potentially affected work order(s)(SDG): 337777
Application Issues:
Failed Recovery for MS/PS
r Specification and Require-ments
Exception Description: -----------
1. The matrix spike 1202990219 does not meet the recovery requirement
due to the matrix of the sample.
Originator's Name:
Maryann Alforque 17 -DEC-13
Page 15 of20
DER Disposition:
1. Reporting results.
Data Validator/Group Leader:
Nat Long 17-DEC-13
DER Report No.: 1252304
Revision No.: 1
l Type:
Process
Client Code:
DNMI
GEL LA BORA TORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: December 19, 2013
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Vegetation Analysis
North East
337777001
SOLID
14-NOV-13 12:00
19-NOV-13
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Pb210, Solid "As Received"
MDC
Lead-21 0 0.000533 +/-1 45E-05 2 27E-05
GFPC, Total Alpha Radium, solid "As Received"
Total Radium 0 000137 +/-3.87E-06 4 71E-06
The following Prep Methods were performed:
Method Description
Dry Soil Prep Dry Soil Prep GL-RAD-A-021
The following Analytical Methods were performed: -------
RL
I OOE-06
5,00E-08
Analyst
LYTl
Project:
Client ID:
DNMI00101
DNMIOOl
Units DF Analyst Date Time Batch Method
uCi/kg KDFI 12/18/13 0920 1348205
uCilkg KDFI 12/15/13 1837 1348207 2
Date Time Prep Batch
11/20/13 0745 1348020.--------
Method Description _____________ _,Anal.==-<-v:::.:st Com men~
I DOE RP280 Modified
2 EPA 900.1 Modified
Surrogate/Tracer Recovery
Lead Carrier
Barium Carrier
Notes:
Test
GFPC, Pb21 0, Solid" As Received"
GFPC, Total Alpha Radium, solid "As Received"
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
Page 16 of20
Result Nominal Recovery,_o/c_o __ A_c_c_,eptable Limits
78.0 (25%-125%)
91,1 (25%-125%)
GEL LA BORA TORIES LLC
2040 Savage Road Charleston SC 29407-[phone]-www.gel.com
Certificate of Analysis
Report Date: December 19, 2013
Parameter
Company:
Address:
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Vegetation Analysis
North West
337777002
SOLID
14-NOV-13 12:45
19-NOV-13
Client
Qualifier Result Uncertainty MDC RL ----Rad Gas Flow Proportional Counting
GFPC, Pb210, Solid "As Received"
Lead-21 0 0.000465 +/-1 17E-05 1 80E-05
GFPC, Total Alpha Radium, solid "As Received"
Total Radium 0.000143 +/-3.70E-06 2.17E-06
The following Prep Methods were performed:
Method Desc~et!_ot_l ::-:--::-:-=--:-=~------
Dry oll Prep Dry oill1rep GL-RAD-A-021
The following Analytical Methods were performed:
Method Description
DOE RP280 Modified
2 EPA 900.1 Modified
Surrogate/Tracer Recovery
Lead Carrier
Barium Carrier
Notes:
Test
GFPC, Pb210, Solid "As Received"
GFPC, Total Alpha Radium, solid "As Received"
l.OOE-06
5.00E-08
Analyst
LYTI
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
Page 17 of20
Project:
Client ID:
DNMI00101
DNMI001
Units DF Analyst Date Time Batch Method
uCi/kg KDF1 12118/13
uCi/kg KDF1 12/15/13
Date Time Prep Batch
11/20113 0745 1348020
Analyst Comments
Result Nominal -'-'--'---'----'----~ Recove~%
99.8
83,8
0920 1348205
1837 1348207
Acceptable Limits
(25%-125%)
(25%-125%)
2
GEL LA BORA TORIES LLC
2040 Savage Road Charleston SC 29407-[phone]-www.gel.com
Certificate of Analysis
Report Date: December 19, 2013
Company :
Address:
Contact:
Project:
Client Sample ID:
SampleiD:
Matrix:
Collect Date:
Receive Date:
Collector:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Vegetation Analysis ---South East
337777003
SOLID
14-NOV-13 13:45
19-NOV-13
Client
Project:
ClientiD:
DNMI00101
DNMI001
Parameter Qualifier Result Uncertainty MDC RL Units DF Analyst Date Time Batch Method
Rad Gas Flow Proportional Counting
GFPC, Pb210, Solid "As Received"
Lead-21 0 0.000592 +/-1.27E-05 I 62E-05 l.OOE-06 uCi/kg
GFPC, Total Alpha Radium, solid "As Received"
Total Radium 0,000118 +/-3.39E-06 2,97E-06 5,00E-08 uCi/kg
The following Prep Methods were performed:
Method Description Analyst Date
;:;,D-I)'""""S,--o"il -;;:Pr_e_p _____ ""'D-I)'--;S;-o-;Cil-;;:Pr-e-p""'G.,-L-;:-RA;-;-;:Do---A-;---;;0;;-21;---------;L-;:Y-;;;T:::-1"------;-;-11120113
The following Analytical Methods w_e_re-'p=-e_r_fo_r_m_e_d_: ------------~
Method Description
DOE RP280 Modified
2 EPA 900_1 Modified
Surrogate/Tracer Recovery
Lead Carrier
Barium Carrier
Notes:
Test
GFPC, Pb210, Solid "As Received"
GFPC, Total Alpha Radium, solid "As Received"
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
Page 18 of20
Result
KDFI 12118113 0920 1348205
KDFI 12/15113 1837 1348207
Time Prep Batch
0745 1348020
Anal st Comments
Nominal Recovery%
107
89.3
Acceptable Limits
(25%-125%)
(25%-125%)
2
GEL LA BORA TORIES LLC
2040 Savage Road Charleston, SC 29407-[phone]-www.gel.com
QC Summary
Contact:
Workorder:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado
Ms. Kathy Weinel
337777
Parmname NOM Sample Qual QC
Rad Gas Flow
Batch 1348205
QC1202990211 337777001 DUP
Lead-210 0.000533
Uncertainty +/-1.45E-05
QC1202990213 LCS
Lead-210 0.0109
Uncertainty
QC1202990210 MB
Lead-210 u
Uncertainty
QC1202990212 337777001 MS
Lead-210 0.0111 0.000533
Uncertainty +/-1.45E-05
Batch 1348207
QC1202990218 337777001 DUP
Total Radium 0.000137
Uncertainty +/-3.87E-06
QC1202990220 LCS
Total Radium 0.00548
Uncertainty
QC 1202990217 MB
Total Radium u
Uncertainty
QC1202990219 337777001 MS
Total Radium 0.00566 0.000137
Uncertainty +/-3.87E-06
Notes:
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
The Qualifiers in this report are defined as follows:
**
<
>
Analyte is a surrogate compound
Result is less than value reported
Result is greater than value reported
The TIC is a suspected aldol-condensation product
0.000483
+/-1.30E-05
O.ol18
+/-0.000152
1.49E-05
+/-4.87E-06
0.0127
+/-0.000158
0.000115
+/-3.75E-06
0.00457
+/-6.03E-05
-1.62E-06
+/-1.12E-06
0.00399
+/-6.74E-05
Units
uCilkg
uCi/kg
uCilkg
uCilkg
uCilkg
uCilkg
uCi/kg
uCilkg
RPD%
9.75
17.3
A
B
BD
c
D
F
H
For General Chemistry and Organic analysis the target analyte was detected in the associated blank.
Results are either below the MDC or tracer recovery is low
Analyte has been confirmed by GC/MS analysis
Results are reported from a diluted aliquot of the sample
Estimated Value
Analytical holding time was exceeded
Page 19 of20
Reoort Date: December 19, 2013
REC%
(0%-20%) KDF1
109 (75%-125%)
109 (75%-125%)
(0%-20%) KDF1
83.5 (75%-125%)
68.1 * (75%-125%)
Page I of 2
Date Time
12/18/13 09:20
12/18/13 09:19
12/18/13 09:20
12/18/13 09:19
12/15/13 18:38
12/15/13 18:09
12/15/13 18:38
12/15/13 18:09
GEL LA BORA TORIES LLC
2040 Savage Road Charleston, SC 29407-[phone] -www.gel.com
QC Summary
Workorder: 337777
Parmname NOM Sample Qual QC Unit~ RPD% REC%
K Analyte present. Reported value may be biased high. Actual value is expected to be lower.
L Analyte present. Reported value may be biased low. Actual value is expected to be higher.
M M if above MDC and less than LLD
M Matrix Related Failure
N/A RPD or %Recovery limits do not apply.
See case narrative
Analyte concentration is not detected above the detection limit
Nl
ND
NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
Sample results are rejected
Analyte was analyzed for, but not detected above the CRDL.
Gan1ma Spectroscopy--Uncertain identification
Gamma Spectroscopy--Uncertain identification
Range Anlst
Q
R
u
UI
UJ
UL
X
y
Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
1\
h
QC Samples were not spiked with this compound
RPD of sample and duplicate evaluated using +/-RL. Concentrations are <SX the RL. Qualifier Not Applicable for Radiochemistry.
Preparation or preservation holding time was exceeded
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more.
Page 2 of 2
Date Time
1\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (SX) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/-the
RL is used to evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
Page 20 of20
ATTACHMENT G
STACK SAMPLE LABORATORY RESULTS
Prepared for:
Energy Fuels Resources
6425 S llwy 91
Blanding, Utah 84511
l)atc of Report:
October 9, 2013
THIRD QUARTER
RADIONUCLIDE EMISSIONS TEST
CONDUCTED AT
ENERGY FUELS RESOURCES
SOUTH YELLOW CAKE SCRUBBER
YELLOW CAKE DRYER BAGHOUSE
BLANDING, UTAH
August 1-2, 2013
by:
TETCO
391 East 620 South
American Fork, UT 84003
. Phone [phone]
Fax [phone] fax
CERTIFICATION OF REPORT INTEGRITY
Teclmical Emissions Testing Company (TETCO) certifies that this report represents the truth as
well as can be derived by the methods employed. Every effort was made to obtain accurate and
representative data and to comply with procedures set forth in the Federal Register.
Dean Kitchen
Re iewer: ~ 7 ?---· ------~~--~~.L------------
Date: ____ --!/-'='t:/'-----lf'-· .-___./~1 __ _
./
ii
TABLE OF CONTENTS
Introduction
Test Purpose ......................................................................................................................... I
Test Location and Type of Process ...................................................................................... !
Test Dates ................................................................ ~ ............................................................ 1
Pollutants Tested and Methods Applied .............................................................................. 1
Test Participants ................................................................................................................... 2
Deviations fron1 EPA Methods ................................................. -.......................................... 2
Quality Assurance ................................................................................................................ 2
Summary of Results
Etnission Results .................................................................................................................. J
Process Data ......................................................................................................................... 3
Description of Collected Samples ........................................................................................ )
Discussion of Enors or Irregularities .................................................................................. .3
Percent Isokinetics ......................................... -. ..................................................................... 4
Source Operation
Process Control Devices Operation ........................................................... -.......................... 5
Process Representativeness ................................................................................... -. ............. 5
Sampling and Analysis Procedures
San1pling Port Location ....................................................................................................... 6
Sampling Point Location ...................................................................................................... 6
Smnpling Train Description ................................................................................................. 6
Sampling and Analytical Procedures ................................................................................... ?
Quality Assurance ................................................................................................................ 7
Appendices
A: Complete Results ru1d Sample Calculations
B: Raw Field Data
C: Laboratory Data and Chain of Custody
D: Raw Production Data
E: Calibration Procedures and Results
F: Related Conespondence
iii
LIST OF TABLES
Table
I Measured Radionuclide Emissions ...................................................................................... 3
II Percent I so kinetics ............................................................................................................... 4
III San1pling Point Location ...................................................................................................... 6
IV Complete Results, South Yell ow Cake Scrubber .............................................. Appendix A
V Complete Results, Yellow Cake Dryer Baghouse ............................................. Appendix A
LIST OF FJGURES
Figure
1 Facility Schematic Representation South Yellow Cake Scrubber ..................... Appendix D
2 Facility Schematic Representation Yellow Cake Dryer Baghouse .................... Appendix D
3 Schematic of Method 5/114 Sampling Train ..................................................... Appendix E
iv
INTRODUCTION
Test Purpose
This test project was conducted to determine the total radionuclide emissions from the South
Yell ow Cake Scrubber and the Yell ow Cake Dryer Baghouse exhausts in terms of Curies per dry
standard cubic foot (Ci/dscf).
These tests were for U-Nat only.
Test Location and Type of Process
Energy Fuels Resources is located about 5 miles south of Blanding, Utah. Uranium ore is
processed into yellow cake, which is shipped to other facilities for additional processing. There
are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the
Yellow Cake Dryer Baghouse. The packaging enclosure also discharges into the Yellow Cake
Dryer Baghouse. The South Yellow Cake (NYC) dryer was the only operating dryer at the time
of the test. The North Yellow Cake dryer is currently not operational. The Grizzly Baghouse
serves as the main dust control device for the raw ore unloading and conveying to the processing
building.
Stack schematics are shown as Figures 1 and 2 in Appendix D.
Test Dates
One test run on the S YC Scrubber began August 1, 20 13 and finished August 2, 20 13. The
second test run on the SYC was completed August 2, 2013.
One run was completed on the Yell ow Cake Dryer Baghouse August 2, 2013.
PolJutants Tested and Methods Applied
The tests were a determination of radionuclide emissions in accordance with EPA Method 5/114.
Test run filters and front wash residues were sent to Test America located in Richland,
Washington for radionuclide analysis.
Test Participants
Test Facility
State Agency
TETCO
Garren Palmer
None
Dean Kitchen
Jeff Graton
Deviations From EPA Methods
None
Quality Assurance
Doug Olsen
Testing procedures and sample recovery techniques were according to those outlined in the
Federal Register and the Quality Assurance Handbook for Air Pollution Measurement Systems,
2
SUMMARY OF RESULTS
Emission Results
Table I presents the findings of the test in Curies per dry standard cubic foot. Tables IV-VI in
Appendix A have more detailed information.
Table I. Measured Radionuclide Emissions
South Yell ow Cake Scrubber Yell ow Cake Dryer Baghouse
Run# pCi/dscf pCi/hr pCi/dscf pCi/hr
1 11.02 8.982E +05 294.7 6.224£+07
2 13.76 1.076£+06
AVE 12.39 9.578E+05 294.7 6.224E+07
Process Data
The process was operated according to standard procedures. All pertinent process data was
available for recording by agency personnel. Scrubber water flow, pressure drop readings ( ~ p)
were recorded and are found in Appendix D. The Dryer Baghouse pressme drop readings (~p)
were recorded and are found on the test run sheets. Production data will be submitted by Energy
Fuels Resources.
Description of Collected Samples
The test filters for the South Yellow Cake Scrubber were heavily covered with a white or pinkish
white colored particulate. The front washes were clear in appearance.
The test filters for the Yellow Cake Dryer Baghouse were lightly colored with a tan colored
particulate. The front wash was clear in appearance.
Discussion of Errors or Irregularities
None
3
Percent lsokinetic Sampling
Each test run was isokinetic within the± 10% of 100% criterion specified in the Federal Register.
Isokinetic values for each test run are presented in Table II.
Table II. Percent lsokinetic Sam lin
Run#
2
South Yell ow Cake Yell ow Cake Dryer
Scrubber Baghouse
96
98
4
101
, . -_. . . -~
I '
• -_.,j._ -..... .&..-:...! ~
SOURCE OPERATION
Process Control Devices Operation
All process control devices were operated normally. Recorded scrubber water flow, pressure and
baghouse t.p readings were recorded and are found on the test run sheets or in Appendix. D.
Process Representativeness
The facility was operated nonnally. Production data was retained by Energy Fuels Resources.
5
SAMPLING AND ANALYSIS PROCEDURES
Sampling Port· Location
The inside diameter ofthe South Yellow Cake Scrubber stack is 12.75 inches. The two, four-inch
diameter sample port are located 28.24 diameters (30 feet) downstream from the last disturbance
and 6.59 diameters (7 feet) upstream from the next disturbance. Figure 1 in Appendix Dis a
schematic of the stack.
The inside diameter of the Yellow Cake Dtyer Bag house stack is 16.0 inches. The two, four-inch
diameter sample ports are located 28.38 diameters (454 inches) downstream from the last
disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample pott
locations are depicted in Figure 2 in Appendix D.
Sampling Point Location
Table III shows the distance of each sampling point from the inside wall according to EPA
Method 1. Each point is marked and identified with a wrapping of glass tape and numbered.
These points are determined by measuring the distance from the inside wall.
Table III. Sampling Point Location
Sample Point
1
2
3
4
5
6
Sampling Train Description
Distance (inches) from Inside Wall
NYC Scrubber Dryer Baghouse
0.85
3.19
9.56
11.90
:~:~··~.~·_.: ·.~.· i,,"4·"·~· • .J
----------. :~:~~~~ .. ~;!·_· _._· _: -~'
0.70
2.34
4.74
11.26
13.66
15.30
To detem1ine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-5/114
were followed.
All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent
interference of the sampled gas and particulate. The stack analyzers used to conduct Methods 1-
6
51114 are constructed to meet the specifications outlined in the CFR. The temperature sensors are
K-type thermocouples. Heater, vacuum and pitot line connections have been designed to be
interchangeable with all units used by the tester. A 316 stainless steel probe liner was used for the
tests. Figure 4 in Appendix Eisa sketch ofthe Methods 5/114 sampling train.
Sample boxes were prepared for testing by following the prescribed procedures outlined in
Methods 5/114.
Sampling and Analytical Procedures
All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A,
Methods 5/114.
Quality Assurance
All equipment setup, sampling procedures, sample recove1y and equipment calibrations were
carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance
Handbookfor Air Pollution Measurement Systems.
7
APPENDIX
A: Complete Results and Sample Calculations
B: Raw Field Data
C: Laboratory Data and Chain of Custody
0: Raw Production Data
E: Calibration Procedures and Results
F: Related Conespondence
8
APPENDIX A
Table IV Complete Results, South Yell ow Cake Scrubber
Table V Complete Results, Yellow Cake Dryer Baghouse
Nomenclature
Sample Equations
A
TABIX IV SYC Strubb('r
COMPLETE RESULTS
Ln~r!_~) Fuels CCJRPORATION, BLANDING. UTA II
SOlri II YELLOWCAKE SCRUBBER EXI tAUS I
Symbol Descri~tion Dimensions Run#l Run #2
Date 8/1-2/13 S/2/ 13
Filter# Xl24 X1~6
Begin Time Test D<:g"n 10:54 17 :01
End Time Test Ended 16:24 23:10
Pb111 Meter Oaromctr ic Prcssmc In Hg. Abs 2<L55 24.55
L'lH Orifice Pressure Drop ln.HP 1.089 1.786
y Metct Calibmtion Y Factor dimensionless 1.000 1.000
Vm Volume GAs Sampled--Meter Conditi011S cf 327.212 324.602
Tm Avg Meier TcmpeHJt\lle "F 86.1 90.8
"1/t-.P Sq Kool Velocity Hc.ad Root in H20 0.5431 0.5210
Wt\\0 Weip;hl Water Colloctou Grams 159.2 548.1
T l Dttration ot Test Minutes 480 360
cp Pilot Tube Coefficient Dim~nsionJcss 0.84 0.84
D, Nozzle Diameter Inches 0.2600 0.3100
C02 Volume% Carbon Dioxide Percent 1.30 ~~.00
0 2 Volume 0/0 Oxygen Percent 17.10 16.90
N2 &CO Volume% Nilro~en and Carbon Monoxide Percent 8 1.60 g 1.10
Vm,,d Volume G"s S:nnplcd (Standard) dscf 260.43:" 256,68<1
Vw Volun1c Water Vapor scr 7.506 25.S43
Bw, (measured) t-raction H,O tn Stack Gas (Measured) Fraction 0.028 0.091
Bw_, (sawated) Fraction H,O in Slack Gas (Saturated) Fraction 0.173 0.168
Bw, fraction H20 in Stack Gas * Fraction 0.028 0.091
xd F1 action of Dry Gas Ftaclion 0.972 0.909
Md Molccul ar Wt Dty Gas lb/lbmol 28.89 29.00
M, Molecular Wt Stack Gas lb/lbmol 28 .:)ll 27.99
%1 Pcn:cnt lsoklnetic Percent 96.1 (17 9 AVG
T, Avg Stack Temperature •r 127.6 \26.5 127.1
A, Stack Cross Sectional Area Sq. Ft 0.887 0.887
Pa Stack Sialic Pressure ln. H20 -0.320 -0.320
Pbr Sample Po1t Bawmctnc Pressure ln. Hg. Al.Js 24.48 24.48
r. Stack Pressure ln. Hg. Abs 24 . ..J56 24.4.56
Q, Slack Gas Volumetric Flow Rate (Std) dscfin 1.36E; 03 UJE :OJ UOE-HU
Q. Stack Gas Volumetric Flow Rate (Actual) cfm 1.901-:-03 I.S4E+O.i 1.87E+03
v, Velocity of Stack Gas fpm 2.15E+03 :: .. OSE+03 :!.J I E+HJ
Curies Radion11Clidcs per smnple pCi 2869.9 3532.0
Crad Concentration of Ratllonuc1ides pCi/dscf [ 1.020 13.76{1 12.3911
ERr ad E1nission Rate ofRadionuc1idcs pCi/hr 8.982E+O:l 1.0 17E-HJ6 9.578E+05
* lflhc measured moisture content is greater than the saturated moisture level (supersaturat~d),
the saturated moisture value will be used in all calculations (40 CFR 60, Method 4. Section 12. I. 7).
Symbol Description
Date Date
Filter#
Begin Time Test Began
End Time Test Ended
Pb111 Meter Barometric Pressure
LJ.H Orifice Pressure Drop
Y Meter Calibration Y Factor
Vm Volume Gas Sampled--Meter Conditions
Trn Avg Meter Temperature
..JLJ.P Sq Root Velocity Head
Wtwc Weight Water Colh"'ted
T 1 Duration of Test
CP Pilot Tube Cocftlcient
Dn Nozzle Diameter
C02 Volwne% Carbon Dioxide
02 Volume% Ox)'!'Cn
TABLE V
COMPLETE RESULTS, PM
DENISON MINES CORPORATION
YELLOW CAKE DRYER BAGHOUSE
Dimensions
In Hg Abs
In H,O
di1nensionlcss
cf
"F
Root ln.
G1ams
Minutes
H10
Dimensionless
Inches
Pet cent
Percent
Run #I
8/2/13
X123
16:25
18:27
24.55
1.576
1.001
105.123
95.3
0.8792
32.2
120
0.84
N 2 & CO Volume% Nitrogen and Carbon Monoxide Percent
0.2220
0.00
20.90
79.10
82.485 Ymsrd Volume Gas Sampled (Standard)
Vw Volume Water Vapor
Bw, f-raction H20 in Stack Gas
Xd Fr:rction of Dry Gas
Md Molecular WI, Dry Gas
M s Molecular Wt. Stack Gas
rYol Percent lsokinctic
T s A vg Sta<:k Temperature
A, Stack Cross Sectional Area
P G Stack Static Pressure
Pbp S<unple Port Barometric Pressure
P s Stack Prcs<trrc
O s Stack Gas Volumcllic Flow Rate (Std)
Q0 Stack Gas Volumetric Flow Rate (Actual)
V s Velocity of Stack (ias
Curies Radionnclides per sample
Crad Concentration of Radionuclidcs
ERrad Emission Rate of Radionuclides
usd'
scf
Fraction
Fraction
lhllbrnol
lbllbmol
Percent
Sq. Ft
In H20
ln. Hg, Ahs
In Hg. Abs
dscfrn
din
fpm
pCi
pCi/dscf
pCi!ltr
1.518
0.018
0.982
28.84
28.64
I 01.4
l18.l
1.396
-0.71
24.48
24.428
3.52E+03
4.81£+03
3.44E+03
24309.0
294.7087
6.224E+07
Drye• O.aghouse. 13
General Nomenclature
%1 = percent isokinetic, percent
A,= (D/ I 4) • 1t
AS~P = see ,J~p
Btu= unit heat value (British thermal unit)
Bws = fraction of water in stack gas (may have designation of "measured" or "saturated")
"measured" represents measured moisture based upon sample volume and water collected
"saturated" is a calculated value based upon stack pressure and temperature
C0 = average of initial and tina! system zero gas calibration bias checks (ppm, percent)
Cav~ = average gas concentration (as measured)
C0 = concentration of particulate matter, back half (gr/dscf,lb/dscf, etc.)
Ccond = concentration of condensibles (grain/dscf)
Coors= concentration of coarse particulate (gr/dsct)
CDor = measured concentration of a calibration gas when introduced in direct calibration mode
Cr.= concentration of particulate matter, front half, actual stack flow (gr /act)
CF = concentration of particulate mCltter, front half (gr/dscf,lb/dscf, etc.)
Cgas = Cavg corrected for initial and final system bias checks (Equation 7E-5)
C.n = average of initial and final system upscale gas calibration bias checks (ppm, percent)
Cma = actual concentration of upscale calibration gas
Cm«al = concentration of metals (ppm, pg/fe, etc.) atomic symbol replaces "metal"
C02 = percent carbon dioxide in the stack gas
cp = pi tot tube coefficient (0.84)
CPMJO = concentration of PM 10 particulate (gr/dscf)
Crad = concentration of radionuclides (pCildsct)
CS = measured concentration of a calibration gas when introduced in system calibration mode
Cx = Any species symbol may replace X. Units may be expressed as ppm, lb/dscf, etc.
Cx (rorrl = actual gas concentration corrected to required percent 02
Curies= Measured radionuclides per sample. Units may be pCi or uCi.
De = jet diameter ( cm)
D/F = Dioxins and Furans (See laboratory report for D/F descriptions and nomenclacture)
~H = orifice pressure drop (inches H20)
~H@ = orifice pressure (inches H20)
~Hd = oritice pressure head (inches Hp) needed for impactor flow rate
Dn = nozzle diameter (inches)
~p = stack flow pressure differential (inches H20)
Dp50 = 50% effective cutoff diameter of particle (em)
D, = diameter of the stack (feet)
EA = percent excess air
ERfl = emission rate of back half particulate (lb/hr)
ERcond = emission rate of condensibles (lb/hr)
ERcors =' emission rate of coarse particulate (lb/hr)
ERF = emission rate of front half particulate (lb/hr)
ER~as = emission rate of a gas (lb/hr)
ERrnrnBtu = emission rate per mmBtu of fuel
ERI'MJo = emission rate ofPM10 particulate (lb/hr)
ER,.d = emission rate of radionuclides (pCilhr)
ERx = emission rate of compound which replaces X. Units are usually in lb/hr.
FD = Dry ba~ed fuel factor. Ratio of the gas volume of the products of combustion to the heat content
See 40 CFR 60, Appendix A, Method 19, Table 19-2 for fuel factor values.
Kc = Cunningham slip correction factor
), = mean free pnth of molecules in gas phase (em)
mmBtu = million Btu
General Nomenclature
Mcond ~ mass ofcondensibles (milligrams)
M cors ~ mass of coarse particulate (milligrams)
Md = molecular weight of stack gas, dry basis (lb/lb-mol)
MF ~ mass of particulate on filter (mg)
MFP ~ mass of particulate matter on filter and probe (mg)
mmBtu = million Btu
M" ~ mass of particulate matter in probe and front wash (mg)
MPMIO = mass of PM 10 particulate (milligrams)
M, = molecular weight of stack gas, wet basis (lb/lbmol)
Mx = mass of species "X". Units may vary and other descriptive subscripts may apply.
!Ls = gas viscosity (poise)
Mwx = molecular weight of gas species (g/gmol)
N = number of jets per plate
N2 = percent nitrogen in the stack gas
0 2 = percent oxygen in the stack gas
'1/f).p = average of the square roots of 6.P (may also be referred to as AS6.P)
'1/c,p 1 = square root of 6.P at point I of the current test, Method 20 I A
'l/f).p 1' = square root of 6.P at point I of the previous traverse, Method 20 I A
'1/{).P'avc = average of the square roots of 6.P from the previous traverse, Method 20 I A
Pb," = absolute barometric pressure at the dry gas meter (inches Hg)
PbP = absolute barometric pressure at the sample location (inches Hg)
Pa = stack static pressure (inches H20)
P, = absolute stack pressure (inches Hg)
P,,d = absolute pressure at standard conditions (29.92 inches Hg.)
e = time of test (minutes)
81 = sample time (duration in minutes) at first sample point for Method 201 A
8" = sample time (duration in minutes) at sample point "n" for Method 20 I A
e,.,,,~ target test time for Method 201 A (minutes)
Qa = stack gas volumetric flow rate (acfm)
Q, = stack gas volumetric flow rate (dscfm)
Q,c = actual gas flow rate through the cyclone (acfm)
Qsce = actual gas flow rate through the impactor (acfm)
Qw = wet stack gas std. volumetric flow ere /min, wscfm)
R = gas constant (21.85 inches Hg*ft'l(lbmoi*R))
p11 = pmiicle density ( 1 g/cm3)
Ps = stack gas density (g/cm 1)
T111 = stack temperature (°F)
T, = stack temperature ( °F)
T5,d = absolute temperature at standard conditions (528°R)
Tt = Duration oftest run in minutes. Also see G
Urn = mean molecular speed (cm/s)
Vm = sample volume (fe) at meter conditions
Vmstd = volume standard (dscf), sample volume adjusted to 68°F and 29.92 inches Hg.
V, = velocity of stack gas (fpm)
V w = volume water vapor (set) at 68°F and 29.92 inches Hg.
Wt.vc = weight of the condensed water collected (grams)
xd = fraction of dry gas
Y = meter calibration Y-factor(dimensionless)
ljf = dimensionless inertial impaction parameter, 0.14
General Sample Equations
2 %1 = Vm,1d • (T, + 460) • I 039 I (8 • V s • P, • Xd • Dn )
As= (D/ I 4) • n:
Bws = Yw I (Ymstd +Yw)
C8 = M8 • 0.01543 I Ymstd
Ccond = Mcond • 0.0 1543 I V lllstd
Ccors = Mcors • 0.01543 I Ytnstd
C,a = T,1d • Crp • P, • Xd I [P,1d • (T m + 460)]
Cr= Mfp • 0.01543 I Ymstd
CpM 10 = MPM10 • 0.01543 IV 111std
C,ad = Curies1Yms1d
CK"' (eorr) = Cgas • (20.9 -desired %02) I (20.9 -actual %02)
c"c DPso = >J [J.lS • \jJ • N • TC • De 3 • I 8 I (Ke • Pp • Osee • 4)]
I o_2o91 I o.1o91 rM,, DPso = 0.15625 • [(T, + 460) (M, • P5)] • (~ls Ose)
ERcond = Ccond • Q, • 0.00857
ERcors = Ccors • Q, • 0.00857
ERF = Cr • Os • 0.00857
6 ERR"" = Pstd • Os • Mwgas • Cgas • 60 I (R • Tstd • I 0 )
ERR"' = Cgas(lb/dscf) • Qs • 60
(Either ERgas equation gives equivalent lblhr values to 3 sig. figures)
ERilllllBIII = cr,as(lb/dscf). Fd. (20.91(20.9-%02), Method 19 Equation 19-1
ERPMIO = CPMIO. Q,. 0.00857
ERrad = Crad • Qs • 60
Kc = I + 2 • A • 1.257 I Dp50
A = J.ls I (0.499 • Ps • U m)
Md = C02 • 0.44 + 0 2 • 0.32 + N2 •0.28
M, = (Md • Xd) + (18 • Bw,)
]Js = [51.05 + 0.207 • (T, + 460) + 3.24 ·10·5 • (T. + 460)2 + 0.53147 • %02 -74.143 • BwsJ • I o·"
P, = PbP +(Po I 13.6)
81 = (>Jt.P1' I >Jt.P'ave) • (8test I pts)
811 = 81 • >Jt.Pn I >Jt.P,
Oa = Ys • As
Q, = Qa • Xd • Ps • Tstd I [(Ts + 460) • P,1d]
Ose = [(T, + 460) • Pstd I (Tstd • Ps)] • [(Vm,,J + Yw) I 8]
Osee = [(T, + 460) • Pstd I (Tstd • P5)] • [(Vmstd + Yw) I 8]
Ow= Q,l x(,
Ps = Ps • Ms • 3386.39 • 10-6 I [R • (Ts + 460) I 1.8]
U 111 = 100 • >J {[R • (T, + 460) I 1.8 • 8 • 103] I [rc • M5]}
Ymstd = Vm • Y • T,1ct • (Pbm + t.H I 13.6) I [Pstd • (T111 + 460)]
V5 = 85.49 • 60 • Cp • ;Jt,.p • >J [(T5 + 460) I (P5 • M5)]
Yw = Wtwc • 0.04715
Xct = I -Bws
APPENDIXB
South Yell ow Cake Scrubber
Preliminary Velocity Traverse and Sampling Point Location Data
Particulate Field Data
Yell ow Cake Dryer Baghouse
Preliminary Velocity Traverse and Sampling Point Location Data
Particulate Field Data
B
South Yell ow Cake Dryer Scrubber
Preliminary S Y Cake Serb
1
Facility Energy Fuels
Stack Identification South Yellow Cake Dtyer Scrubber
A Date tf( -9._/ h
I N Barometric Pressure
Pbm in Hg PbP in Hg
B --1 Static Pressure (P0) in H20
Estimated Moisture (Bw.) 4-6 %
Sample Height from Ground 70 feet
Comments:
Stack Dia, 12.75" Reference: 0"
Ports arc 7' Upstream from next disturbance
Ports arc 30' Downstream from la~t disturbance
Traverse Percent Distance From: Ports
Point Diameter ID Reference A B c D E F
1 6.7 0.85 0.85 tel> I""~ " -J~O .C(
2 25.0 3.19 3.19 /I.JS-. ~;,-lo 1-.. ~~ ..
3 75.0 9.56 9.56 /u (.. ·1.0 101-.(,AJ
4 93.3 11.90 11.90 lo~ .j,Q IO ?-' / ·"$
Averages:
Ts LFlow
~p .J~p
•
KEY=> ITs LF!owl
~p
~b ~ !l·'t Mlb~
Filt~r ~ Sarnyl_e Bo:<~
>'\ t 2. s %/"J.f r':>
_____ Field Data Sheet
Plant: Energy Fuels
Date. %/~ J \ ';
Location: South Yellow Cake Dryer Scrubber
Operator jt;Ff GQ.~'"\O'hl
~· ---
Traverse Time DGM 6P tl.H (mH,OI Vacuum Temperatures ("F1 DGM T~mpiTm/
Polnt Clock Min (6) •.Jll [inl/lO) Desired Actual (iTIIfg) Stack (T,) Probe Probe out Oven Effluent Out In
1~ \o·.S'"l 0 ~fa,'\.53 \~ ._32. Lu~ ~~no ~~· i2.~ 2.1.a~ 2.(,.,~ 'J.b<o LSc 1'-i ll
1 2.e b'\~.io\~ .n L~e ·., . ~ ('. 3 t ':l, -1 2S~ 'l'"'H 2."1 ~ ~5 !S _"'lq
1 ~() I, 0., ., ,.,-.32 \, \O \ \(1 3 i'l. '1 l.loS 1.~2. 2,1..,.2_ 1,.,.5. aS ....aL..
2 ~Q li~2.l 't~4 • ~2 \. \o l. ~(I ,!, 12.4 -2. ~ Lt 2'1~ 2...t•i0 ~ ~..s 1<::t ~~
2 Re, 1~ \'0~ .~'1 ~.~~ Li~ ..... i2.'i k_"it. 2.Lf3 %~3 1oS 9.n ~
2 aoo l!t;O .1. '2. S ,3,4 L\'1 LU'i ~ \25 2~5 'l.SO 7.5o lc.O 9.~ ~1
3 -i2.o li....~.35o .3~ ~ ~~ Lo~ ~ \'2.5 J.~S 2.~0 2Jaa s~ ~,-g~
3 u'io i#i.4'-i1 .~\ \.~'1: La'"\ ~ ~2~ 2!1iS. :1-'iS '2:-i ;:._ '51 %\ ' %4 t 3 lr;:!~ H •. o r~c:;.~o . ~~ i, c'i ~ o111 3. i. '2.4 2.~S 'l'f1 'L~i ~ <'i!l ~l.l ., ~~ 4 1![ :o2. \'i\o ~~-:z . ~'l.T .'2.0i .'\{l .97! 3. i2.~ 2.bO 2~5 2~5 io"1 __ai. g:/_
_____L 2oo 1 ~ "? ~'is .2.S .'6~~ .S~\ ~ \2-B 2~0 2.5~ 25!!! ioi S2 is
~ 4 12.2..0 ~?_c. '\qro._ .2.$ ''ill-'3 \ ·'-~i 3 e'LP. 2.~7 2.t'oo 2\.oO loS ~~ ·~
1 L2:2'i ·:2~() .~~S.-rH . 2.., • '\ 1.:!'-i .~b~ ;; t;o 12~~ 25-b_ 2.Sb_ ~L &5 ~,
1 %.o 21o0 1Xs9 . ],i'1 .2.~ ,'\\o't ,ql.p'i 5 h'2..~ 1~55 2.ldi 2..b'i bs a <a ,0
1 'ill 2~0 ~2 Cf1S 27 .~~t> .%1:\~ 5 l'3c 12..5~ "2.J,k "2,(gfo, ~3 %Co qo
2 laO .~ -B&_5_9~1.... .2.6 .~~i. • 5'.qQ. r '.a ~~~ 2.S2 "2.1,, 2bl loS ~~ (\~
2 __bo 320 IS~~. o\aS. .'2.~ .£l2\ .~2~ (-. u~! 2(ob 2.S~ '2,.~~ toto qo c;s
2 'io -:z.'i~ 1"112.. ~'i4 ·2'l .~'2..\ .~2i (o i~C> 2-Sb 2.&.1~ 2'iq 62. '\o ~~
a L.c ~leO l'l'-~!.\~8 • 1-9 .~i~ .~i'"i ., \30 2So 2'15 2Lf5 1.:,2, C{, 1'1 4
3 2o ~B6 '\3d\ ~in1<t .2.ct ,(\/~ .91~ ., f~\ 2So 2Afh 12'-t~ b2 &'l !:13
3 _!It>. lfoo '\S3. S2.1 ·ltO ,qlfo .~&fo ·~ 17. '\ 21.to 2."15 1 2.~5 ~3 I "'0 115
)l#C\~"1 ol"l4 h o l42.o C\~11 0"2., ·2C& ·~"io -~&.\o co ]~ 2Jii'::.( 2.S! 251 ~j Cil,l 9_5
4 Zo r.4'f 0 'l~.J.Co U .'2,.~ ·~ ~() • tt ~() ~ ~~ 2S% 252.. 252 (o! Dti <:tl...
4 liD. ['ib_O -q9 ci t!fo .~fi il , G'i I 11 o'il ~ ~~Q 12So 1-SS 255 to\ '12 cr/
bo I "tao \<':l!OE!>. O\lo
-
lr~.o~a, r~~~ ;T'~ v .J c; "~l?;. .7 CL ~0 iHa .. -~" -·-1~19\b /
Average
2Dcf.i~lj o-S~l! o.9;(.
32-i , ~11. -.10, sw_'<~-./ L o~q )<~'" l2~. 2. ,/ a4.7 .to 1\o.~ /
Additional (Extra) Leak Check Information
DGM before Leak Check Vac ("Hg) Rate (fe/minl A-vt .... /.... · _c;-c; D Z-0 • 01) .?
-'}-C."---~7~1.1 7 _ _) {)i) s
't: Slri'.J"r \)o~ t~·:~S -C.:t:.~-rQ.f:l""\11"~& te~N • .)~
S"fAe."'r \If-' : ~I: o2.. 'h. A~
DGM After Leak Check Vac f'Hg)
Page ___Lor_\_ Run # _l_
r .-() N
StackDiameter 12.75" Port Reference --"0'--"---
Ports are 7' Upstream from next disturbance
Ports are 30' Downstream from last disturbance
Assumed Moisture 4-6 %
Probe ~ Cp 0.84
Nozzle Calibration
• 2i'oo • 2.<12o ~ • 2.bO
Avg D. , 2!o0 inches
Gas Bag(.-0]
Console_~_.·, __
Y-Factor ~. (l)~e
6H@ l I ~'l e in H,O
Barometric Pressures
Pbm 2 "7 • 13$ in Hg
Pbp 2 ~ . '{ ~ in Hg
PG ~ , 3 L in H,O
Leak Check. Pre J>osr
ft'lmm o,oo~ ~-<6~~
vacmllg 2.:2. 'c
..)~d.O
0-003
~3
PitctRate 0., G65" o.Q o.o
lnH,O~-s.~ Ci.o
..k:. S-o
Water Collected ~ s~ .L g
J~ Ttme Sampled ~~i~Go min
'i !3~ Review S+$-:5'
K= @T,
Sfo.! K= @Tn,
Rate (fe/min)
~~~. i,"1 ~
~
____ Field Data Sheet
Plant: EnerCJy ~els
Date: g {:V :!>
T.-:1verse Time
Point Clock Min (9)
1 5:c\ 0
1 -,s
1 30
2 -If c. ...
2 uo
2 i5 -rs-
3 30 "to
3 &IS cos-
3 ~ j'tc.;>
4 ,s 1?6'
4 3o lS""O
4 o1S ((,5
1 2D:i0ioo t~O
1 1!5 t'i\
1 Jo 'L~D
2 ~ '2-'t-~
2 b:l 'Z,....(,()
2 15_ 'Z,S"'5
3 :!» 'I-~
3 If~ ~fJJ
3 c..t "JbO
4 ~s 1-;c~
4 30 r,;o
-l'?u,-, 4 '1S
~'3!-\o£..o r-;~ou
DGM
•ill}
OOtV\'10
:o1. \,2.s ~
0~~ .1\b~
lo" S._ 10'2..5
,oS~ o\S
l!ll~. 'lor.;
lo~ "'3. "l'i~
,~!.,SS
H \ _15<"1 5.
l'2.S. t4 I,
.\";,i.\c-36
l.&.t ~ .'l\~
n,~.2..1<o
\11 ~~3.
!q2 oH ...
..., o_k ~St;,
'2t.o. l22.
2'!>"l-2tU
2 't ll ";'}j)
21c2.-~S'S
2llD S'l1
2q~ \h 0
'"!.o 'i a.i1S
~l'i. ~~5
'53"-1. ~b'i
6.P ~H !n'IH,OJ VJcuum
(i:.H~O) Desired Actual {illH.g)
.2.'2. \ ·""'0 L"'..,o "3
.2'2. i .fofo l .&~~o 4
.12. ! ~'{Q Vi&4o s
. 22. i '1~% l.~qg s
~2.~-\, S\ 1.4 i.Sl"\ ~
2.~ ! 5.\~ i ,1;1"\ ' .2\ __ q, ~~3 1.~'!3 J .
• 2.~ \. 9\ ~'2 !.q~3 <\ .2'\ . \,~q~ L~'' uo
• '2. \ \ .'315 L!.IS \2,
"l.S i .~sl \.~~., ~0
·25 i IA'l,, U .... o;.""'l fl ...
.2<ll ILC,.oo J.1oo -4
.3o I i .<\~'i i.~\.,"l 5
·~0 \,Oj~o,~ L ,b'i b
·3o L~'i .t~. f
z,o ID,9.t.,"t l.q~-,'1 %
• s__o_ \ .9kH b .~IQ'i ~
• 2... '\ 'k ,()0 n .~o() te
.2~ l.C=too ~.~_l) H
,?_/ \ "1(oil i,lt..% 1"2-
.~3 2 .h ... ~ 1'2.M iL.
.'3,(o 4_."!.51 2.351 ~to\
,3,4. 2 .c"tt:. 2.o,c qb
~ . 1 TETCO .,z
Filter t Z U' Sample Box_'/ __
).12."1
Location: South Yellow Cake Dryer Scrubber
Operator Je~f ~"'fqh\
Temperatures ~~-J DGM 'fcmp(T .. I
Stack (T,) Probe Probe out Oven Eflluent Out In
12., 2.3o 2.3o 2St~ {oo C\'2.. '\~
l2~ 2."!$ ~~5 2C:,O 1..-~ t\2.. <t,
n'l.~ 2~'5 2~'5 'l.&;o b.o tt3 9S
l'!>o l_2_'f0 2&fo £..55 Joo 9'3t ~a
\2.~ '2.4. 0 _2"'10 2;S l.oO '\'; q~
\ '2.~ 'l.t.;S L.•iS 2155 oO q2 '\~
i'L~ :2\S 2-iS 2~'5 '1ft ~b ''~ -i2B 2So 2.'50 2.50 Lo '\o C\b
~"2.~ 1 250 2So 2So '-16 ~~ _35_
q2.(D 2~~ 2521 ':l.loo ~0 ~" 111_
a'l."6 '2b~ 21.:.~ 12-n '\5 ~~ ~:;
fl,./ 2S'i 2So 25o ~~ S<i\ ~5
tll 2.~ 2~0 2."10 ia_S ~ ~9
i2...~ 23o 2'-io 12'fo bs ~s ~~
~2, 2'io 2.So '2-So 53. &5 q::,
i.'l.! 2&t~ 2'15 2.is. S3 165 ~~
ll.l 2'fo 2'!S 2.'1S 5S ~ C1s
~ '2...:1 2_ijo .24_5 2~S sc; '6'i 't"3,
~2~ 2.~~ 2'fS 2.'i5 c;s, ~q 93
a2.1 I'Lt.fS 2So '2£;0 5_-S ~"' !.9c~
!2S 12So -:2, ss 2SS 5~ ~li ,~
~20 2S~ 2SS 255 ~Q ~3 q ~
fi2o 2So l.So l..St~ lo4 Bi 6~ nq '2.SO 2J.o0 '2.1oO foS. /1'1 '6&
Total 'J'Zd .(!C>"L-"1 ~ .so'-\3 '-lL·~<i 103~ 1>~&
q C>• <6 Average
~ <:.\...-.. ... -s~
~n4.,.,.~
" -SZIO J-'1-~(p r -z, &.S>
Additional (Extra:) Leak Check Information
DGM before Leak Check Vac ("Hg) Rate (te/min)
!(a3.27<.o \\o o.ooS \(a~ .1 03 B o.oo~
~ .
•
DGM After Leak Check Vac ("Hg)
Page _l__of+ Run#~
-
r
A .o N
Stack Diameter 12. 75" Port Reference __,0:...." __ _
Ports are 7' Upstream fiom next disturbance
Ports are 30' Downstrea_m from last disturbance
Assumed Moisture 4-6 %
Probe J.1 (p Cp 0.84
Nozzle Calibration .;t-o ~ .:2!:0 .'$ll>
,,.g 0;, T ?! D :f.C:h!IS
Gas l3a~ _L::l?._ _
Courot~~
Y · f:lCIOT, [ ~ 0 t;.G-
:\H,,. l .'{_ Zl.Oh1 H,O
Sarom~uic Pic:SS'Jr.:S
Pb"' '2.<-\ • '; 5' m Hg
PbP "Z q "'i.. ~ in 1-Ig
Po-( -'3 "2.. in H20
Leak Check:
~7 ~
fi'lmin 0 .OQ~
l!lli.
o .oo'-__ __,,
vac in Hg 4.,'!;. 2"\
PitotRate 0.0 ~
[nH10 ~ ~
Water Collected SiS . Y ~
Rate (ft3/min)
Time Sampled mtn
Review
K=
K=
@T,t
@T,.
Yell ow Cake Dryer Baghouse
Prelim 6 pts blank
Facility Energy Fuels Resources, Blanding, lJT
Stack Identification N01th Yellow Cake Drvcr Baghouse
Date
I Baromctl"ic Pressure
B Pb111 in Hg Pb, in 1-lg
0 N Static Pressure (PG) in H20
A Estimated Moisture (Bw,) I %
Sample Height from Ground feet
Comments:
Sl;ll'k Dia 16 Ret<"ence 0
Ports are 57" Upstream from ni'Xt disturbance
Ports are 468" Downstream from last d istUI bancc
Traverse Percent Distance From: Ports
Point Diameter ID Reference A B c D E F
I 4.4 0.70 0.70
2 14.6 2.34 2.34
3 29.6 4.74 4.74
4 70.4 11.26 11.26
5 85.4 13.66 13.66
6 95.6 15.30 15.30
Averages:
Ts L'Flow --------
t.P __ _ -.Jt.P ----
KEY=>
rJ\ ) F1eid Data Sheet
Date:
Trav~rsc Time
PcP11
1
2
3
4
5
6
1
2
3
4
5
6
y 11 -t:., TETCO (\
Filter_'\, _(L.L_. Sample Box_~~ t __ \ Page --1.......0f__,... Run!! __
Location: Yel~ke Dryer Baghouse
Operator: ~~ • l
DGM ~p Temperatures (l'J DGM T;::mp.(t,.)
i B
.() N
(1\') !.LnH~) Stack {T,) I Probe I Probe Out I Filter I Effluent II Out I In
J( v I L.:SDIZ.i. D_l ~<tV I~'-[ II >c,t.-I~~
Stack Diameter 16"__ Port Reference _0,0"_
Pi>rts are 57" Upstream from next disturbance
---'---l~l 1 • 9. ~ 1 •, . l!JI! •• lf--:?.L--l Ports are 468" Downs1rean1 frum ~!lit dl!rutlunu
Assumod 1\.~obrure. b 1 ~~
Probe / ~ Cp 0:84
Nozzle j:al ibration '( "? 7 -z. t,_ . U..'L '1.-'Z-• ~vv -7.,
AvgD,~mches ----
Gas Bag Ambt~l Alr
C11ns<>lc S Y-F~tor~ I
'I' v-·vv_, U---j ~ t!Ho l-'{~ \ rnH20
I
I
/ II I /
Baromerric PressuJl'-'
Pbm (.. <-\. q ~ 1n Hg
Pb, c19 '{ '? ioHg
PeL.'_ ' ( in H20
Loak Ch.c< &!;. f<ls
ft'imin 0 00} Q · DO ~
vac in Hg Z. "l;, ....:11....\~--
rl ,_.,
Pilol Rare (/ • V
lnH,O~
o· s.c; J
Water Collected ~ '7 • Z/ . L g
Time Sampled ~ \ l () min
Total I o £ .\L-? ~ tv·~so"\ ~ C/1-\ 7 l L{ (i v Review ~ \
--· ..
/1 ~ /11
" , & --r~ \ · 5 ;:rv ll Sr ·l C1{·) A'w:~
K~ @Tn.
K ~ ran.
Comm~nts Time Bag house 11.P Time Baghousei1.P I 1{;~1'; tii -7 &-10 \D· I :~ ( ,~l ~ s ·.(~ () I D· ~ u lrr \ /'io' e ·:::r. / '1' I LA \ ~ ·.2_"0 I0-7 v
. "0 (.}. v_ _l~ ,1_.;-
South Yell ow Cake Scrubber
Sample Recovery
Gas Analysis Data (ORSAT)
Yell ow Cake Dryer Baghouse
Sample Recovery
Gas Analysis Data (Ambient)
Chain of Custody
Lab Analysis
APPENDIX C
c
South Yell ow Cake Dryer Scrubber
METHODS
Facility: Energy Fuels Date: --------
Stack Identification: SYC Scrubber ~~~~~------------------------
IMPlNGERS
lMPINGERS
JMPINGERS
Run:
l
~lrop out
'
Run:
dr pout .
Sample Box:
2
Lupgcr Number I 3 I _!. I 5
Initial Volume of liqu id (l llO) i11 IIIIJiingcr . (ml)
Sample Box:
lmpingct· Number
I.LI..!.Ii
lnitlnl Volume ofliquid (H20) in impingers, {ml)
roo I drop om I 1 oo I
lo21.S 5 1·
6
Silica Gel
/
e \
(
6
Sili1:aGel
Initial (g) ..::....::...!....--':=--fT--..:...><-:...,u---f-':...l-.:...:;...~..p;.l:():.,..__l _D_. -'-~;_-t-s_·. _3_<-.-=-. -~--1----:--,---;'­
Net (g)=!=!::!:::~=::::::!::::!:~===:!::::====::==::!:::=:!==============::::::!::::::!:!:::!::::=
Run:
..L
Sample Box:
lmpinger Number
:z I 3 I 4 I ..a...
Initial Volume ofliquid ~,_0) in impingers, (ml)
100 .I drop out I I 00 I
'
Total (gl
-=======~==-----
6
Silica Gel
lMPINGERS
Run: Sample Box:
l.mpmgcr Number
...L I ..L I 4 I 5 6
Initial Volume of liquid (H20) in imping ·rs, ml)
drop out 100 I drop out I I 00 I Silica Gel
' '
Final (g) ___ --+----1-----t---___,1------+----
lnitial (g) ----+----+----+-------ii-----1-----
Net(g) ======~====~========================
Total (g) ======
r
Plant_ '·~ e "1 --1 Location. ___ S_'{_L _________ _
Analytical Method. ___________ _
~ _.)
D"'~
TestNo. Z.....
Gas Bag No. {r 0 'J..
!ti Ambient Temp
Operator
Date -----
Test No.-----
Gas Bag No.-----
Ambient Temp-----
Operator ____ _
·'-'
Gas
0 2 (Net is Actual 0 2
Reading Minus Actual
C0-2 Reading).
N2 (Net is 100 Minus
Actual 0 2 Reading).
Gas
C02
0 2 (Net is Actual 0 2
Acnool
Reading
Actual
Read in~
2.-D
Net
I
Net
'Z.A)
RUN
Actual
Reading
2
\J. I
RUN
2
Actual
Reading
2..-o '
Net
Net
Z..o
Reading Minus Actual If?·, ~~-cr 18"-~ C02 Reading). 1~-'i.
N2 (Net is 100 Mitlus ~-~:~.~~:· I,,:' ~1[
Actual 0 2 Reading). jiJ -0 <,q ~~~ .:,...,:o
RUN
I 2
Arlual Net Actual Net
Ga~· R~adin~: Reading
coz
0 2 (Net is Actual 0 2
Rending Minus Actual
C02 Reading)
N1 (Net is 100 Minus ~~~~1 ' .. -n Actual 0 2 Reading). . ·. ?fl:~ J
t 0 2 was determiued using a gas aualyzer
CO is not measured, as it has the same molecular weight as N2
3
Aclual
Reading
I. ,
1~.,~·-.
Afhlal
ReJtdiu_g
z...o
lB-·1
~~~~:.:~
i\dual
Ruding
3
3
r~ '· --~
~'·
Net
f, ~-1 _.../
Nrt
Z..o
1(, ·1
Nd
Average
Net
Volume
Average
Net
Volume
Z·O
/(.,7
Average
Net
Volume
Yell ow Cake Dryer Baghouse
NYC Baghouse MS
Facility: Energy Fuels
Stack ldentification:..:.N.:....Y:...C:::....=B:.:::iag;;::h.:.::o:.::.u:.::se;__ ___________ _
lMPINGERS
IMPfNGERS
---IMPINGERS
Final (g)
Initial (g)
Net1g)
Final (g)
Run: Sample Box: -4=
lrnpinger Number
2 I ~ I -!-I s 6
lnlt.inl Volume ofliqu1d (H20) in impingers, (ml)
JOO I 00 I I Silica Gel r . ' ' . ·' {
(p /ct . L/ ';.)D3-=!-5<:-z!. ~ ~fl.)
(., '~·" Go~tf. (p ~ztP.s 'i''1, .l
( o.·z~ q. I 3'-/ Zo·c_
_./
Total (gJ==~=-a-=.,...=~=~=-s=z · ·z:..
Run: Sample Box:
bnpinger Number
.!. ...L I --L I ....L I 5 6
Initial Volume of illttiid (I I10) in lntping,crs, (ml)
100 100 I I SilicaGcl I
----~~----4----+-----+-----~----
lnitial (g) ___ --li------4----+----+---~----
Net (g)====!===::::!:===='====:::!::===:::!:::===
Total (g)========
Run: Sample Box:
lmpingcr Number
I -...LI..LI....LI 5
Initial Volume of liquid (H,O) in impingcr$ (mO
I 00 100 I I Silica Gel I .
Final (gl -----~~---4----~----+---~----
lnitial (gl ___ -11------4----+----1------1-----
Net (g) =====~====~====~====~====~======
Total (g) ======
IMPINGERS
Run: Sample Box:
lmpinger Number
.l-l...l...I....LI.2..
lnilinl Volume of liquid (H20) in lmphll!.trs, (ml)
Final (g) -----~----4-----+----+---~---
Initial (g) ___ _, ___ -+----l-----1----+---
Net(g) ==================~====~====~=====
Chain of
Custody Record
li'J._-c. ~· (!IJOZi
Client
Tetco
Address 391 East 620 South
City American Fork
~le.."f Narrre .and L.watiOn (SJalaJ
r~: r;:~~3
Energy Fuels 2013 3rd Quarter
Temperature on Receipt __ _
Drinking Water? Yes 0 No 0
PrQiect MatJaaer
Dean Kitchen
T(!.'!(pfu:>ti:!;,N~ (Ar~ Cada)ilf.l§l.< tfurrt>or
801-492-9106
Site Contact ] Lab Contact
Scott Christensen, Garntn Palmer
Carrier/Wsybi/1 Number
Test America
THE LEADER iN ENVIRONMENTAL TESTING -Date Ghaiil' ol CuS!!JrJrl NurnW!Y-
8/05/2013
Lab N!Jml1<rr I I Page of
Analysis (Attacl'l list if
more space is needed)
Special Instructions! ~ui'l:III!SiiO{QR/O<tt>leNo. Containers & 0 Conditions of Receipt Matrix Preservatives 0 "' ~ ~ "' N
l g ":' N "Q
Sample 1.0. No. and Description ~ i 5 tl~ :1: .. "' Date Time } 'ti :& "' ~ :::> .... a: .s (Contain11rs for each sample may be combined on one line) ·"' J! ~ ~ ~<: ..;
R1 Dryer BH filter (X123I and beaker 8/2/13 16:00 X I X
R1 SYC Scrubber filter (Xl24,12S) and beaker 8/1,2/13 8:00 lx I X
R2 SYC Scrubber filter iX126,127; and beaker 8/2/13 15:00 X X
'
I -
1 I -..
! I 1
..
I
~bf9Ha;tllfd IIID(Irifl~n J $i=pfe OfsrxJ:sat · ~~~Lab (A fee ma.v be assessed if ssmpf<iS af9 l'>teined 0 Non-Hazard 0 Flammable 0 Skin lrritar.t 0 PoisooB 0 Unknown 0 Retum To Client 0 Arctr/ve For ___ Moolhs longer than 1 month) --QC R<lijuTII!lT!OnlS, (SpeCifl)
0 TDays O 14Days 0 21 Days 'hr;r a.s_Re.r m~!i
l .wn~ 12~ T. R.r;r.ii!i$11 Sy ~jj IT""" I ~te" / I Trm~· r2· Rec8/i{IJIJ 8y =-------1 D.xte I Ttma
:L Re.'lnquisl!eu By
1
Da:te J Tmm 13. Re<:eM!d' By
1
earS: j rrme
C<Xr.meniG
When Complete Email to: Dean or Paul [e-mail]
DISTRIBUTION: WHfTE-Relumed ro Clienl withReport; CANARY-Stays with lt!e Sample; PINK-Field Copy
SDGNo. Order No.
47154
TestAmerica Inc
rptSTLRcbTitle v3.73
TestAmerica Laboratories, Inc.
Analytical Data Package Prepared For
Denison Mines (USA) Corp.
Radiochemical Analysis By
TestAmerica Inc
2800 G. W. Way, Richland Wa, 99354, (509)-375-3131.
Assigned Laboratory Code:
Data Package Contains 14 Pages
Report No.: 57059
Results in this report relate only to the sample(s) analyzed.
Client Sample ID (List Order) Lot-Sa No. Work Order Report DB ID
R1 Dryer BH filter J3H090411-1 M1LAX2AA 9M1LAX20
(x123)and b
R1 SYC Scrubber J3H090411-2 M1LA81AA 9M1LA810
filter(x124, 12
R2 SYC Scrubber J3H090411-3 M1LCA1AA 9M1LCA10
filter(x124, 12
Batch No.
3224041
3224041
3224041
Test America
THE LEADER IN ENVIRONMENTAL TESTING
Certificate of Analysis
September 23, 2013
Denison Mines (USA) Corp
1050 17th Street, Suite 950
Denver, CO 80265
Attention: Dean Kitchen
Date Received at Lab
Project Name
Sample Type
SDGNumber
I. Introduction
August 8, 2012
Energy Fuels 2013 3rd Quarter
Three (3) Stack Filter Sample
47154
CASE NARRATIVE
On August 8, 2013, three stack filter samples were received at TestAmerica's Richland laboratory for
radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification numbers
as described on the cover page of the Analytical Data Package report form. The samples were assigned to
Lot Numbers J3H090411 .
II. Sample Receipt
The samples were received in good condition and no anomalies were noted during check-in.
III. Analytical Results/Methodology
The analytical results for this report are presented by laboratory sample ID. Each set of data includes
sample identification information; analytical results and the appropriate associated statistical
uncertainties.
The analysis requested was:
Alpha Spectroscopy
Uranium-234, -235, -238 by method RL-ALP-004
Tes!America Laboratories, Inc. 2
Denison Mines (USA) Corp
September 23, 2013
IV. Quality Control
The analytical result for each analysis performed includes a minimum of one laboratory control sample
(LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments"
section.
V. Comments
Alpha Spectroscopy
Uranium-234, 235, 238
Sample Rl Dryer HB Filter (Xl23) and Beaker had a FWHM above acceptance limits. The sample was
stripped from the disk, reprocessed and recounted. The recount is now within acceptance criteria. The
achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to historical
process knowledge. The sample activities exceed the MDAs. Data is accepted. Except as noted, the LCS,
batch blank and sample results are within acceptance limits.
I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically
and for completeness, for other than the conditions detailed above. The Laboratory Manager or a
designee, as verified by the following signature has authorized release of the data contained in this hard
copy data package.
Reviewed and approved:
Erika Jordan
Customer Service Manager
TestAmerica Laboratories, Inc. 3
Drinking Water Method Cross References
DRINKING WATER ASTM METHOD CROSS REFERENCES
Referenced Method lsotope(s) TestAmerica Richland's SOP N
EPA 901.1 Cs-134, 1-131 RL-GAM-001
EPA 900.0 Alpha & Beta RL-GPC-001
EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002
EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002
EPA 903.1 Ra-226 Rl-RA-001
EPA 904.0 Ra-228 RL-RA-001
EPA 905.0 Sr-89/90 RL-GPC-003
ASTM D5174 Uranium RL-KPA-003
EPA 906.0 Tritium RL-LSC-005
Results in this report relate only to the sample(s) analyzed.
Uncertainty Estimation
TestAmerica Richland has adopted the internationally accepted approach to estimating
uncertainties described in "NIST Technical Note 1297, 1994 Edition". The approach, "Law of Propagation
ofErrors", involves the identification of all variables in an analytical method which are used to derive a
result. These variables are related to the analytical result (R) by some functional relationship, R = constants
* f(x,y,z, ... ). The components (x,y,z) are evaluated to determine their contribution to the overall method
uncertainty. The individual component uncertainties (u;) are then combined using a statistical model that
provides the most probable overall uncertainty value. All component uncertainties are categorized as type
A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the
components, such as sample homogeneity, are combined with the component uncertainty as the square root
of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result
is the combined uncertainty (uc) multiplied by the coverage factor (I ,2, or 3).
When three or more sample replicates are used to derive the analytical result, the type A
uncertainty is the standard deviation of the mean value (S/?n), where S is the standard deviation of the
derived results. The type B uncertainties are all other random or non-random components that are not
included in the standard deviation.
The derivation of the general "Law of Propagation of Errors" equations and specific example are
available on request.
TestAmerica Inc
rptGenerallnfo v3. 72
Tes!America Laboratories, Inc. 4
0.
Action Lev
Batch
Bias
COCNo
Count Error (#s)
Total Uncert (#s)
Uc_Combined
Uncertain(v.
(#s), Coverage
Factor
CRDL (RL)
Lc
Lot-Sample No
MDCIMDA
Primary Detector
Ratio U-234m-238
Rst/MDC
RstffotUcert
Report DB No
RER
SDG
Sum Rpt Alpha
Spec Rst(s)
Work Order
Yield
TestAmerlca Inc
rptGenerallnfo v3.72
TestAmerica Laboratories, Inc.
Report Definitions
An agreed upon activity level used to trigger some action when the final result is greater thun or equal to the Action
Level. Often the Action Level is related to the Decision Limit.
The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed
together.
Defined by the equation (Result/Expected)-I as defined by ANSI N13.30.
Chain of Custody Number assigned by the Client or TestAmerica.
Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same
units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background.
All known uncertainties associated with the preparation and analysis of the sample are propagated to give a measure
of the uncertainty associated with the result, Uc the combined uncertainty. The uncertainty is absolute and in the
same units as the result.
The coverage factor defines the width of the confidence interval, 1, 2 or 3 standard deviations.
Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmerica "default"
nominal detection limit. Often referred to the reporting level (RL)
Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
associated with the sample. The Type I error probability is approximately 5%. Lc=(l.645 *
Sqrt(2*(BkgmdCnt/BkgmdCntMin)/SCntMin)) * (ConvFct/(Eff*Yld*Abn*Vol) * IngrFct). For LSC methods the
batch blank is used as a measure of the background variability. Lc crumot be calculated when the background count
is zero.
The number assigned by the LIMS software to track samples received on the same day for a given client. The
sample number is a sequential number assigned to each sample in the Lot.
Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
with a Type I and II error probability of approximately 5%. MDC = ( 4.65 *
Sqrt((BkgmdCnt/BkgmdCntMin)/SCntMin) + 2.71/SCntMin) * (ConvFct/(Eff * Yld * Abn *Vol)* IngrFct). For
LSC methods the batch blank is used as a measure ofthe background variability.
The instrument identifier associated with the analysis of the sample aliquot.
The U-234 result divided by the U-238 result. The U-234ru-238 ratio for natural uranium in NIST SRM 4321 C is
1.038.
Ratio of the Result to the MDC. A value greater than 1 may indicate activity above background at a high level of
confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers
associated with the result.
Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of2 a value greater than I may
indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence
interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers
associated with the result.
Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order
Number.
The equation Replicate Error Ratio= (S-D)/[sqrt(TPUs2 + TPUd2)] as defined by ICPT BOA where S is the original
sample result, Dis the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the
total uncertainty of the duplicate sample.
Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt.
The sum of the reported alpha spec results for tests derived from the same san1ple excluding duplicate result where
the results are in the same units.
The LIMS software assign test specific identifier.
The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method.
5
Report No. : 57059
Client ld
Batch Work Order Parameter
3224041 FFSR
R1 Dryer BH filter (x123)and b
M1LAX2AA U-234
U-235
U-238
R1 SYC Scrubber filter(x124, 12
M1LA81AA U-234
U-235
U-238
R2 SYC Scrubber filter(x124, 12
M1LCA1AA U-234
U-235
U-238
No. of Results: 9
Sample Results Summary
TestAmerica Inc
Ordered by Method, Batch No., Client Sample ID.
Result+-Uncertainty ( 2s) Qual Units
1.16E-02 +-1.9E-03 uCi/Sample
6.09E-04 +-1.5E-04 uCi/Sample
1.21 E-02 +-2.0E-03 uCi/Sample
1.42E-03 +-5.0E-04 uCi/Sample
3.99E-05 +-3.3E-05 uCi/Sample
1.41 E-03 +-5.0E-04 uCi/Sample
1.67E-03 +-5.3E-04 uCi/Sample
2.62E-04 +-1.1 E-04 uCi/Sample
1.60E-03 +-5.0E-04 uCi/Sample
Date: 23-Sep-13
SDG No: 47154
Tracer
Yield MDL CRDL RER2
83% 3.59E-05 9.00E-15
83% 2.47E-05 9.00E-15
83% 4.30E-05 9.00E-15
94% 4.73E-05 9.00E-15
94% 2.97E-05 9.00E-15
94% 5.01 E-05 9.00E-15
91 % 5.01 E-05 9.00E-15
91% 3.10E-05 9.00E-15
91% 4.07E-05 9.00E-15
TestAmerlca Inc RER2 -Replicate Error Ratio= (S-D)/[sqrt(sq(TPUs)+sq(TPUd))] as defined by ICPT BOA.
rptSTLRchSaSum
mary2 V5.2.24
A2002
TestAmerica Laboratories, Inc. 6
Report No. : 57059
Batch
Work Order Parameter
FFSR
3224041 BLANK QC,
M1LMK1AA U-234
U-235
U-238
3224041 LCS,
M1LMK1AC U-234
U-238
No. of Results: 5
QC Results Summary
TestAmerica Inc
Ordered by Method, Batch No, QC Type,.
Result+-Uncertainty ( 2s) Qual Units
3.04E-08 +-1.6E-07 u uCi/Sample
4. 57E-08 +-1.1 E-07 u uCi/Sample
1.52E-08 +-1.1 E-07 u uCi/Sample
7.22E-06 +-1.6E-06 uCi/Sample
6.1 OE-06 +-1.4E-06 uCi/Sample
TestAmerica Inc Bias -(Result/Expected)-I as defined by ANSI N13.30.
Date: 23-Sep-13
SDG No.: 47154
Tracer LCS
Yield Recovery Bias MDL
95% 4.51E-07
95% 2.49E-07
95% 3.62E-07
89% 104% 0.0 2.78E-07
89% 84% -0.2 2.67E-07
rptSTLRchQcSum U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or
mary V5.2.24 not identified by gamma scan software.
A2002
TestAmerica Laboratories, Inc. 7
Lab Name: TestAmerica Inc
Lot-Sample No.: J3H090411-1
FORM I
SAMPLE RESULTS
Client Sample ID: R1 Dryer BH filter (x123)and b
SDG: 47154
Report No. : 57059
COC No.:
Parameter
Batch: 3224041
U-234
U-235
U-238
No. of Results: 3
Result
FFSR
1.16E-02
6.09E-04
1.21E-02
Comments:
Count
Qual Error ( 2 s)
5.0E-04
1.1E-04
5.1 E-04
Total MDL, Rpt Unit, Yield Rst/MDL,
Uncert( 2 s) Action Lev Lc CRDL(RL) RstJTotUcert
Work Order: M1LAX2AA Report DB ID: 9M1LAX20
1.9E-03 3.59E-05 uCi/Sample 83% (321.8)
1.07E-05 9.00E-15 (12.4)
1.5E-04 2.47E-05 uCi/Sample 83% (24.7)
5.02E-06 9.00E-15 (8.2)
2.0E-03 4.30E-05 uCi/Sample 83% (281.3)
1.42E-05 9.00E-15 (12.4)
Ratio U-2341238 = 1.0
Date: 23-Sep-13
Collection Date: 8/2/2013 4:00:00 PM
Received Date: 8/8/2013 10:55:00 AM
Matrix: FILTER
Ordered by Client Sample 10, Batch No.
Analysis,
Prep Date
9/19/13 06:00 p
9/19/13 06:00 p
9/19/13 06:00 p
Total Sa
Size
1.0
g
1.0
g
1.0
g
Aliquot
Size
0.0012
g
0.0012
g
0.0012
g
Primary
Detector
ALP6
ALP6
ALP6
TestAmerica Inc MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
V5.2.24 A2002
TestAmerica Laboratories, Inc. 8
Lab Name: TestAmerica Inc
Lot-Sample No.: J3H090411-2
FORM I
SAMPLE RESULTS
Client Sample ID: R1 SYC Scrubber filter(x124,12
SDG: 47154
Report No. : 57059
COC No.:
Parameter
Batch: 3224041
U-234
U-235
U-238
No. of Results: 3
Result Count
Qual Error ( 2 s)
FFSR
1.42E-03 1.7E-04
3.99E-05 3.0E-05
1.41E-03 1.7E-04
Comments:
Total MDL, Rpt Unit, Yield Rst/MDL,
Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert
Work Order: M1LA81AA Report DB ID: 9M1 LA81 0
5.0E-04 4.73E-05 uCi/Sample 94% (30.1)
1.66E-05 9.00E-15 (5.7)
3.3E-05 2.97E-05 uCi/Sample 94% (1.3)
7.72E-06 9.00E-15 (2.5)
5.0E-04 5.01 E-05 uCi/Sample 94% (28.2)
1.79E-05 9.00E-15 (5.7)
Ratio U-2341238 = 1.0
Date: 23-Sep-13
Collection Date: 8/2/2013 8:00:00 AM
Received Date: 8/8/2013 10:55:00 AM
Matrix: FILTER
Ordered by Client Sample ID, Batch No.
Analysis,
Prep Date
8/30/13 10:59 a
8/30/13 10:59 a
8/30/13 10:59 a
Total Sa
Size
1.0
Sample
1.0
Sample
1.0
Sample
Aliquot
Size
0.0012
Sample
0.0012
Sample
0.0012
Sample
Primary
Detector
ALP3
ALP3
ALP3
TestAmerica Inc MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
V5.2.24 A2002
TestAmerica Laboratories, Inc. 9
Lab Name: TestAmerica Inc
Lot-Sample No.: J3H090411-3
FORM I
SAMPLE RESULTS
SDG: 47154
Report No. : 57059
Client Sample ID: R2 SYC Scrubber filter(x124, 12 COC No.:
Parameter
Batch: 3224041
U-234
U-235
U-238
No. of Results: 3
Result Count
Qual Error ( 2 s)
FFSR
1.67E-03 1.8E-04
2.62E-04 7.2E-05
1.60E-03 1.8E-04
Comments:
Total MDL, Rpt Unit, Yield Rst/MDL,
Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert
Work Order: M1LCA1AA Report DB 10: 9M1LCA10
5.3E-04 5.01 E-05 uCi/Sample 91% (33.4)
1.85E-05 9.00E-15 (6.4)
1.1 E-04 3,1 OE-05 uCi/Sample 91% (8.5)
8.98E-06 9.00E-15 (5.)
5.0E-04 4.07E-05 uCi/Sample 91 % (39.3)
1.38E-05 9.00E-15 (6.3)
Ratio U-2341238 = 1.0
Date: 23-Sep-13
Collection Date: 8/2/2013 3:00:00 PM
Received Date: 8/8/2013 10:55:00 AM
Matrix: FILTER
Ordered by Client Sample 10, Batch No.
Analysis,
Prep Date
8/30/13 10:59 a
8/30/13 10:59 a
8/30/13 10:59 a
Total Sa
Size
1.0
Sample
1.0
Sample
1.0
Sample
Aliquot
Size
0.0014
Sample
0.0014
Sample
0.0014
Sample
Primary
Detector
ALP4
ALP4
ALP4
TestAmerica Inc MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSample U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
V5.2.24 A2002
TestAmerica Laboratories, Inc. 10
Lab Name: TestAmerica Inc
Matrix: FILTER
Count
Parameter Result Qual Error ( 2 s)
Batch: 3224041 FFSR
U-234 3.04E-08 u 1.6E-07
U-235 4.57E-08 u 1.1 E-07
U-238 1.52E-08 u 1.1 E-07
No. of Results: 3 Comments:
Total MDL,
Uncert( 2 s) Lc
FORM II
BLANK RESULTS
Rpt Unit,
CRDL Yield
Rst/MDL,
RstiTotUcert
Work Order: M1LMK1AA Report DB ID: M1LMK1AB
1.6E-07 4.51E-07 uCi/Sample 95% 0.07
1.52E-07 9.00E-15 0.38
1.1 E-07 2.49E-07 uCi/Sample 95% 0.18
5.06E-08 9.00E-15 0.83
1.1 E-07 3.62E-07 uCi/Sample 95% 0.04
1.07E-07 9.00E-15 0.27
Ratio U-2341238 = 2.0
SDG: 47154
Report No.: 57059
Analysis, Total Sa
Prep Date Size
8/30/13 10:59 a 1.0
Sample
8/30/13 10:59 a 1.0
Sample
8/30/13 10:59 a 1.0
Sample
TestAmerica Inc MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
Date: 23-Sep-13
Aliquot Primary
Size Detector
0.11 ALP5
Sample
0.11 ALP5
Sample
0.11 ALP5
Sample
rptSTLRchBiank U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
V5.2.24 A2002
TestAmerica Laboratories, Inc. 11
Lab Name: TestAmerica Inc
Matrix: FILTER
Count
Parameter Result Qual Error ( 2 s)
Batch: 3224041 FFSR
U-234 7.22E-06 1.1E-06
U-238 6.10E-06 1.0E-06
No. of Results: 2 Comments:
FORM II
LCS RESULTS
SDG: 47154
Report No. : 57059
Total
Uncert(2 s) MDL
Report
Unit
Expected Recovery,
Yield Expected Uncert Bias
Work Order: M1 LMK1AC Report DB ID: M1 LMK1 CS
1.6E-06 2.78E-07 uCi/Sample 89% 6.95E-06 3.62E-08 104%
Rec Limits:
1.4E-06 2.67E-07 uCi/Sample 89%
Rec Limits:
75 125
7.28E-06 3.79E-08
75 125
0.0
84%
-0.2
Analysis,
Prep Date
8/30/13 10:59 a
8/30/13 10:59 a
TestAmerica Inc
rptSTLRchLcs
V5.2.24 A2002
Bias -(Result/Expected)-I as defined by ANSI Nl3.30.
TestAmerica Laboratories, Inc. 12
Date: 23-Sep-13
Aliquot
Size
0.14
Sample
0.14
Sample
Primary
Detector
ALP6
ALP6
~ en s;
3 <D 5· Ql
I; rr 0
Cil Q
Cii"
"' 5" ,
w
Chain of
Custody Record
TAL-4124(1007)
~,
Tetco
Temperature on Receipt---
Drinking Water? YesO ·NoD
r=;~ l D~~n Kitchen
Test America
THE LEADER lN ENVIRONMENTAL TESTING
-
I ~snn13
~--_j ii!leuhrJil'J ~(AI!!i!,CCdeliF-ii!Nf!II1k!;J: J.eb NtiiJiiHv 391 East 620 South 801-492-9106 I -
Ci!Y I American Fork l~Sblte i i~CodP .. ·Site Cantact I Lab Contact Ana~s (Af!e~
.I Ut I .840Q~ ~ Smtt:Christensen, Ga11"811 Palmer moreS/)aCS'IS ·
' ....
r-P~Pt~!H.I Canier/Waybifl Number I t:rlerw Fuels 2013 3rd Quarter I I
~-~No.
Matrix Containers & s Preseniatives I ~ C> ~ ·~ m
t ~ N
Sample I.D. No. and Description ~ "' a ~a ;5 .;, Date Time l ~ ;g ~ ~ "' .3 (Contair>e1s for each sample rrr.ry be combined on one litre] ~ :S ! ~ ~~ II.-r R1 Dryer BH fi)ter(X12~) and beaker 8/2/13 16:00 X X .. _ l J
18/1,2/13 lx I l Rl SYC Scrubber filter (Xl24,125) and beaker ~ _x I i
R2 SYC Scrubber filter (l(l.26,1271 and beaker 1 8/2/13 115:00 LX.i .X l
l ~J
I --:<\'""'-~ ~ :\. CJ
~,-<., ~V'\n'-4 IJ .. J ~' I
1 G\...-e ~£:....,-Sl..., ! i i__l = lit 111m' lllllllllllllllllllll J3 090411 -
--··-~-·-.......... . .. I
I .Chsin of CsJSIDdv. Number
Page l of I
-
Special InstructionS!
Conditions of Receipt
'\V\\L~-1-
\(V"\ \ ( ~~
M\LC,~
r
f'o;ssible P.a:«mm~ I Samp/a.Dispos<?l 1J!1 fee may b6 ~if ssmpfes al\"1 rf11ained 0 ~Hazard D Flammable D Skin Jrri!ant 0 Poison B · 0 Unlmovm 0 Relwn To Client t;(.Dfsposar sy Lab 0 An:flive For __ Months longer than 1 tr:ontl1)
-~ ff«iu!re;;iiiit$ ~
0 7 .Deys 0 14 Da}S 0 21 Da}'S
.~\:\\9_~<J.L ~~
-2.
3. By aRI!Cii.!lVeaBy
Coo'71mllfl)l; I When "Complete Email to: Dean or Paul tetco@tetcO,.ut.com . -bJSTRIIJiiT10it WHITE-ROO!med rc Oi!enJ will) Ropott CANARY • S1eys. W11h rfll) Ssmpf2; PINK· .J'"ItJJd CGyiy
Test America Sample Checl<:-in List
Date/Time Received: ~-SS-Yb \ c:>SS TH" LOADER Iff ENVIRONMENT A" TESTING ~
Container GM Screen Result: (Airlock) L\\) cpm .Iuit.it~l •
Sample GM Screen Result (Sample Receiving) ~ cpm Jnit.i'als
Client: SDG #:_~~-·1'\--!.\..:...S""'. M:.......J_ ____ sAF #: ________ _:
Lot Number: ~~ D'--\ \\
ChainofCustody# _____________________________________ _
Shipping Container ID or Air Bill Number : _______ --r _____ NA ~ J
Samples received inside shipping container/cooler/box ] Continue with 1 through 4. Initial appropriate response.
] Go to 5, add comment to #16.
No [ No Custody Seal' ]
No [ No ~tody Seal l ]
___ °C NA r)
Wet,[ ) Dry' J
1. Custody Seals on shipping container intact? Yes [
2. Custody Seals dated and signed? Yes [
3. Cooler temperature:
4. Vermiculite/packing materials is NA[
Item 5 through 16 for samples. Initial appropriate response. ~
5. Chain of Custody record present? Yes 1 No [ ]
6. Number of samples received (Each sample may containmu iplc bottles):_~~--------------
7. Containers received: ~·'~~i..P.-ea;..c...:"D..,._,"--'m'--'--!.l\ ...... """\oo~"'.a.~..k.x.ML£~------------
8.
9.
10.
11.
12.
13.
14.
15.
16.
Sample holding times exceeded? NA [ Yes [ No¥ ]
ample have: __ tape __ hazard labels __ custody seals appropriate sample labels
Matrix: ~·. A (FLT, Wipe, Solid, Soil) __ I (Water) ___ S (Air, Niosh 74 0) __ 1' (Biological, Ni-63)
amples:r
are in good condition __ are leaking __ are broken
have air bttbb\o (Only for samples requiring no head space) __ Other __________ _
Sample pH appropriate for analysis requested Yes [ ] No [ ] NA~ ]
(If acidification is necessary go to pH area & document sample ID, initial pH, amount of ~l added and pH after addition on table)
Were any anomalies identified in sample receipt? Yes [ ] No [ ~]
Description of anomalies (include sample number'8').;-NA ~
Sample Location, Sample Collector Listed on COC? *
*For documentation only. No corrective action needed.
Yes[ ]No~]
Additional Information:._.!..;~4-~-------------------------------
] Client/Courier denied temperature check. ] Client/Courier unpack cooler.
Sample Check-in List
Signature: _____ '>"i,....,___.._.,___,....,.....,...""""' _________ Date:._.-_......::......;:..-. ___ _
] No [ Date:
By:
Person contacted: [ }d No action neceSsnry; process as is
Project Manager c ~'-q 1.W!.l::::=:==:..__Date CZ-9-l ~
LS-023 Rev. 17, 05/13 Page 1 ofj
TestAmerica Laboratories, tnc. 14
APPENDIXD
South Yellow Cake Scrubber
Figure 1. Facility Schematic Representation
Yell ow Cake Dryer Baghouse
Figure 2. Facility Schematic Representation
Process Data
(Retained by Energy Fuels Resources)
D
Fadlity Energy Fuels Resources
t
a
t
y
stackidentification: South Yellow Cake Scrubber
l+---0 __.,
~
a: Distance upstream from next disturbance, feet 7' -------------------
~: Distance downstream from last disturbance, feet }()'
65' y: Distance of Sample Level to Ground, feet ------------------
0: Stack Inside Diameter, inches 1 ?_ 75" ----------------
Estimated Moisture, percent 4-8
100-120 Estimated Temperature, °F -----------------
Estimated Velocity, fpm 3.000
Control Unit
Type:
Scrubber
'1 "-Number of Ports
~
Figure I. Facility Schematic Representation
Process
Type:
Yelltm Cake Processing
Focility Energy Fuels Resources
t
a
!
y
Stack Identification: yellow Cake Dryer Baghouse
1._0 __..I
13
a: Distance upstream from next disturbance, inches 57" --------
13: Distance downstream from last disturbance, inches 454"
y: Distance of Sample Level to Ground, feet 65'
0: Stack Inside Diameter, inches 16"
Estimated Moisture, percent o-:~% ..
Estimated Temperature, °F 1::!5 --------------
Estimated Velocity, fpm I ,400
Control Unit
Type:
Baghouse
Number of Ports 2
+
Figure 2. Facility Schematic Representation
Process
Type:
Yellow Cake Pmccssing
Energy Fuels Resources, Blanding, UT Process Data
Source: South Yellow Cake Date: $; / /,"">
Scrubber Flow GPM
Time #1 ~ L\P
to:;o 3 {)· '-( 1-D-}
7o .L( \ r 0·~ t r : DO \
l I : ~0 ~u -~ l [D·1 I
~: ()cJ }0·7 I 1 O-T
I Z: ) t> "3 0 . L-( I {6·1-
IS: D 0 3u L ( \ t u ·-:f
l ~ ·~ )0 -,o ."J ( 0 ·1
-+~~~~rro '?10· -"t f ro·-:1
.. ,~: 3o 3 ():<-( (u -~ /
/'0 ..
,.J,Jf : oc.:> ·> o ~_I ) I ,.., ··1
I I / c....-· I 1-
I ,~,· 7 n 1._./. ~ .......
t-<"· ) 0 -; c ( I ' _J .. I I •.
t \ . -
.}"tf t>O ~ , ,. /I ' ~ .. ·r ( f (') --t (_
~· 3 0
.
\ f -(
;:.' , .j
~ ( ) -l 2 ..
~ "'2. • <:, I ~ , I ·. () 0 •V l -! 3
.f_#: . 3o 2' I ., .. f ;· --:f . , ) . ' :• I ,_.). ,
.J-!r-~ ()0 -s [).) I I .-; ,:( . : (j . /.
-~ )o '2 f ~··~{ ' ;;;c) ·· '-r I , .. ( I/ I . /· '·'
.{4 ~0 ·?.'I "" r c) / !
f( ;A ... , lj
/
Jf) , . .3() ") () . \ '0 ' (
1': ·'/
./
i It;. oo ) ~. 7 ... ( cl· !-
I l? -~ /--... )D·'"S /I \!) I
c/ t_,. -r-'
..1 .. •
Energy Fuels Resources, Blanding, UT Process Data
I
----· I ,' -· ~r · '\ Source: South Yellow Cake Date: i)' l
Scrubber Flow GPM
_,
\ Time #1 #2 t>P
r:t-6u ·?_ '1. &-.) ! J--*)' 1--I I J
( ....-1 ··I
t-:}-5o L ~'C-) lo 1-I I
~{) L~
, i -! { &~ OD ~-
·:;,u.-6 I ~.(,
I ~ '!;O i
(.)(/ -!f~:;o 1/ I ~~-\ ~~ ~.0 ' i'\ ·""I
i --r ·-( \ ' --I
'0~ I
\ . -.. r-;t\ ~· (
?uoo <'-" I I ., "' l I
l~-\ ' ----, 5-'2 t) $o I -t ·
Zl OD 1-c\, CZf r+ ·>
z I ~ [l ).C). D I 1 's-·
? I) ' I l I -1 ')-'Zl. I) C. '
?Z 3V )0 '\ (~1-<)
1.-~ ()L:> 1()' () r1·)
Z 3'· ,5D )0 -c) r1· )-
I
I
APPENDIXE
Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature
sensors were carried out in accordance with the procedures outlined in the Quality Assurance
Handbook. The appropriate calibration data are presented in the following pages. The nozzle
calibrations are recorded on the first page of the field data sheets.
Figure 3 Schematic of Method 5/114 Sampling Train
Meter Box Calibration Data and Calculations Forms
Post-test Dry Gas Meter Calibration Data Fonns
Type S Pitot Tube Inspection Data
Sample Box Temperature Sensor Calibration
E
Temperature Sensor
t .~Probe
TypeS Pitot
Tube
Temperature
Temperature
Sensor
lmpingerTrain Optional, May Be Replaced Bt An Equivalent Condenser
j Temperature
Sensor
Nozzle · 1-ta:Tra:Jld
sensor~ Goosene. ck I ~--------------
lmpingers
~ Gas&lired
/ Ftcl:e ---
/
TypeS Pitot
Tube ~
Stack
Wall
Glass Filter
Holder
Manometer Temperature Water
Sensors
Orifice
Empty Silica
Gel
Air-Tight
Pump
Figure 3 Schematic of Method 5/114 Sampling Train
IT.;)
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
G
G
G
1) Select lhree critical orifices to calibrate the dry gas meter which bracket the expected operating range
2) Record barometric pressure before and after calibration procedure.
3) Run at tested vacuum (from Orifice Calibration Report), for a period of lime
necessary to adlieve a minimum total volume of 5 cubic feet.
4) Record data and information in the GREEN ceUs, YELLOW cells are calculated.
METER SERIAL -~1 .. ... I
CRITICAL ORIFICE SET SERIAL•: 14535 EQUIPMENT ID #:
RUN#
2
2
3
K'
FACTOR
(AVGI
0.9137
0.6137
0.8137
0.5317
0.5317
0.5317
0.3307
0.3307
0,3307
TESTED
VACUUM
lin Hgl
1l
13
1l
13
13
13
13
13
13
645.607 6SZ.11S
652.115 658.605
ssa.6os 665.066
602.003 j .607.609
613.065 I 618.569
618.669 I 62>1.268
628.000 633.184
633,184 838.396
638,396 o43.&26
6.508
6,490
6.461
5.606
5.604
5.599
5.1e4
5.212
6.230
71
71
71
69
6!1
69
71
71
71
78
79
79
73
74
75
72
73
76
79 84
79 67
79 87
74 75
75 76
75 77
73 76
76 80
76 80
87
87
87
76
77
78
80
80
80
FINAL
[ 25.20-j
ELAPSED
DGM TIME(MIN)
AVG a
AVG(P,.,I
25.20
2013 Pre-Calibration
IF Y VARIATION EXCEEDS 2.00%,
ORIFICE SHOULD BE RECALIBRA TED
l
8Z ~ 5.3407 0.99Z 1.526
83 5.3564 5.3407 0.997 Yll.
83.00 5.3325 5.3407 ~ ~
AVG = .2J.ll .:Qd!!
74.50 ·B.OJI § U!J!. ~ 2,ill !.ill
75.so s.oo o 4.6696 urn o.ns 1.ll!
76.25 8.00 0 4.&589 Mill .!.Qru. M!i
AVG= 0.998 ~
75.00 12.00 4.3149 4.3411. ~ ~
77.25 12.00 4.320 4.3411 ~ 1.425
78.00 12.00 0.40 4.3289 4.3411 ~ ~
AVG• .!&n ~
USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
The Mowing equations aie used to calculate the standard volumes of air passe<! thnJ(I!Ih the DGM, V0 (std), and the crifical orifrce,
v. (std). and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y ~I 1.000 I
AVERAGE 6H~ ~I 1.490 I
(1)
(2)
(3)
~~m,_.,..,_. = K, •Vm"" Pbar+(/).1{1}3.6)
Tm
Pbar_.':("J_ vcr . .,,,, = K'• ··'..iramb
= Net vok.Jme of gas sample passed through DGM. corrected to standard conditions
K1 = 17 64 ;R/Jn Hg {English). 0.3858 °KJmm Hg (MetricJ
T..., = Absolu:e OGM avg temperature \R • En~lish. 01K -Metric)
~ Volume of gas sample passed through the critical orifice, corrected to standard conditions
Tomb= Absolute ambient temperature (0R-English. ~K-M!!tric)
K' = AYe rage K' far;tor from Crit1cal Orifice CalibratiOn r·ci:,,.J, )' ~ --
1'111, .. ,..
= DGM calibration factor
lee aa:h
Al"'\bient A1r
Soiling Water
2 6Ha = ( 0.75 9 ) !IH (V,(std))
V.,(std) v.
T2mperature Sensors
Reference In Out
OF
33
62
202
'F
33
62
203
'F
33
62
203
PRE Console #4 Calibration 2013
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Select three critical orifices to calibrate the dry gas meter Which bracket the expected operating range.
2) Record barometric pressure before and after calibration procedure
~ '"' 9-~"'-_.,,,,,
3) Run at tested vacuum {from Orifice Calibration Report), for a period of time
necessary to achieve a minimum total volume of 5 cubic feel.
4) Record data and information in the·.<:~:::'' cells, YELLOW cells are calculated.
METER SERIAL f!l oo••• I
CRITICAL ORIFICE SET SERIAL II: 1453~ EQUIPMENT 10 ~:
K' I TESTED
r--------r----~FACTORIVACUUM
G
G
G
RUN~ I (AVG)
2
)
2
~
0.8137
0.8137
0.8137
0.5317
0.5317
0.5317
O,U07
0.3307
0.3307
(inHg)
12
12
12
1J
13
13
20
20
20
128.204
133.568
139.020
95.7570
100.951
106.479
111.900
117.108
122.338
USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
133,58! 5.384 ro n
139.020 5.432 ro ~
144.448 5.428 ~ "
100.951 5.194 70 69
106.479 5.528 70 70
111.698 5.219 70 70
117.108 5.208 70 74
122.339 5.231 70 75
127.555 I 5.220 70 75
~
~
~
70
70
73
75
76
n
n IM
Ml~
" I~
6' 71
71 72
72 75
75 76
76 77
77 78
INITIAL
~ G
79.75
86.25
89.50
69.75
70.75
72.50
75.00
76.00
76.75
FINAL AVG(P,.,J I 25.45 I 25.45
ELAPSED I
ITIME~MINJ
7.50
8.00
7.50
§ 0
0
12.00
12.00
12.00
4,5144
~
4.4705
~
4.6936
4.4167
4.3778
~
4.3736
2013 Pre-Calibration
IF YVARIATION EXCEEDS 2.00%,
ORIFICE SHOULD EIE RECALIBRATED
~
4,4990
4.4990
AVG~
4.4097
4.7036
4.4097
AVG=
4 3881
4.3883
4 3883
AVG=
i.ill:
.bll.!!R.
1.006
UQ1
!Mi!!.
~
!Mi!!.
~
1.002
.wmt
1.003
1.002
l
w
-1).12
0.11
till
!.ill
1M!
!,ll!
!.ill
!:ill.
M1.!
.Llli.
1.lli
The fonowing equations are used lo calculate the standard 110lumes of air passed through the DGM, v. (sld], and the Olitko! orifice,
V" (std) and /he DGM calibration iactor, Y. These equations are automalically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 1.001 I
(1)
(2)
(3)
Vm"''"; K, •I'm• PharTt/Mf 113 6)
Tnt
Pbal' • El_
Vcr, ·~') = K'• .JT;mb
:Net volume of gas sample passed through DGM, corrected to standard conditions
K, = 17 64 'R/in Hg (EngliSh), 0 3858 'Kimm Hg (Metric)
T.,.,:::. Absolute OGM avg, temperature (0R-Cnglish, aK-Metric)
= Volume of gas sample passed through the critical oriiice, corrected to standard conditions
r .. ~ = Absolute amb•ent temperature CR-English "K-Metric)
K' = Average K' factor from Crilical Onfice Calibratior.
f'cti .. ,J. r---= DGM calibration factor -:·m,,;,.
AVERAGHHe=i 1.481 :J
> 6Hg = ( 0.75 9 ) 6H (Vm(std))
V"(std) Vm
Temperature Sensors
Reference tn Out
OF CF OF
32 J3 32
72
203
73
202
73
202
Pre 2013 5 ::onsole
METHOD 5 DRY GAS METER CALl BRA TION USING CRITICAL ORIFICES
1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range
2) Record barometric pressure before and after calibration procedure.
3) Run at tested vacuum (from Orifice Calibration Report), for a period of time
necessary to achieve a minimum total volume of 5 cubic feet.
~~ -$~ a:, !O!IMQIIIAJl&bW ----__ ., -
I• .
4) Record data and information in the GREEN cells, YELLOW cells are calculated.
METER SERIAL #:1 ~• w• I
CRITICAL ORIFICE SET SERIAL •: 14535
K' TESTED
FACTOR VACUUM
RUN# (AVG) (in Hg)
l.:l:~ ~ LJ 3 t!±=j C±=j
G: 0.5317 13
0.5317 13
0.5317 13
38.903 44.153
44.153 49.395
4S.395 54.655
G· 0.6808 13
0.6808 13
0.6808 13
59.15200 64.567
64.567 70.000
70.000 75.427
USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
.0
.0
.0
5.250
5.242
5.260
5.415
5,433
5.427
EQUIPMENT ID #:
F 1-I I I I
I 83 BZ 83 84 86
I 84 83 84 86 88
I 84 84 85 68 90
85 I 85 86 89 91
as I 86 86 91 95
85 I 86 87 96 98
DGM
AVG
0
0.00
83.7$
85.25
86.75
87.75
89.50
91.25
'
Facility:
FINAL AVG (P...-)
I 25.45 I 25.45
ELAPSED
TIME(MIN)
e
§§
§r----'1
50
50
0
1.10
§ 00
4.3506
4.3322
4.3352
~
4.4656
4.4465
Energy Fuels
SYC
IF Y VARIATION EXCEEDS 2.00%,
ORIFICE SHOULD BE RECALIBRATED
AVG=
4.3565
4.3525
4.3525
AVG~
4.4543
4.4543
4.4543
AVGs
1.001
.tQM
1.004
~
0.998
0.997
1.002
.Q,ill
l
0.22
.:Q,ll_
1.,lli
1.518
1.514
1.599
1.,ill
~
The following equations are used to calculate the standard volumes or air passed through the DGM, V m (std), and the critical orifice,
V ~ (std), and the DGM calibratkm factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 1.001 I
(1)
(2)
(3)
Vm.,,d, = K, • Jim* Pbar+ (Mf /13.6)
Tm
Pbar * 0 Vcr,,.;, = K '* -JTamb
= Net volume of gas sample passed through DGM, corrected to standard conditions
K, ~ 17 64 'Riin Hg (English), 0 3858 'Kimm Hg (Metric)
T m ~ Absolute DGM avg_ temp9rature ('R -English, 'K-Metric)
= Volume of gas sample passed through the critical orifice, corrected to standard conditions
T a~rJ) = Absolute ambient temperature ClR-English, °K .. Matric)
K' = Average K' factor !rom Critical Orifice Calibration
VCI(stl() Y = --= DGM calibration factor
Vmr.r'"' Icc Sath
Ambient Air
Boilins;~ Wa!er
AVERAGE !lH!!J =( 1.556 I
2
t.Hii!l = ( 0.75 a ) !lH (V.,(std))
V«(std) v~
Temperature Sensors
Reference In Out
OF OF OF
33 33 33
52 62 62
202 203 203
Post Console #4 Calibration 2013
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.
2) Record barometric pressure before and after calibration procedure.
lis wwwmg-.. ---'~ ~;---~~ 4: ; . •
3) Run at tested vacuum (from Orifice Calibration Report), for a period of lime
necessary to achieve a minimum total volume of 5 cubic feel
4) Record data and information in the GREEN cells, YELLOW cells are calculated.
METER SERIAL i/:1 ----~ I
CRITICAL ORIFICE SET SERIAL Ill! 1453S EQUIPMENT ID II:
K' TESTED
r--------.----~ FACTOR I VACUUM
RUN ti l (AVG) (In Hg)
o:rn~ .O F I II fl .O
.0
G: 0.5317 13
0.5317 13
0.5317 13
23.402 29.735
29.735 35.3a2
35.382 40.693
6.333 as 82 83 82 as I
85 83 as 85 so I
L__~ 65 87 9~-~j
5.647
5.311
o:rn ~ .0
I T Fl-[ I .0
.0
USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
INITIAL
DGM
AVG
0.00
0.00
0.00
83.00
85.75
89.00
0.00
0.00
0.00
FINAL
[ 25.35 [
ELAPSED
TIME (MIN)
B
AVG(P.,,)
25.35
§§
§ 00
50
§§
~
~
4.3422
Energy Fuels
Dryer Baghouse
IF Y VARIATION EXCEEDS 2.00%,
ORIFICE SHOULD BE RECALIBRATED
1
AVG=
5.1977 0.993
4.6202 0.995
4.3314 0.998
AVG= 0.995 ]!,QQ.
AVG=
1.533
1.526
!.ill
The following equations are used to calculate the standard volumes of air passed through 111e DGM, V m (std), and the critical orifice,
V~ (std), and the DGM calibration factor, Y. TheSil equations are automatically calculated in the spreadsheet above AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = l----o.9~
(1)
(2)
(3)
Vm,,d> = K, * Vm * Pbar .._ (b.H /13.6)
Tm
Pbar * 0 Vcr,,d, = K'* .JTamb
= Net volume of gas sample passed through DGM, corrected to standard conditions
K1 = 17 64 "Riin Hg (English), 0 3859 °Kimm Hg (Metric)
T m = Absolute DGM avg. temperature ("R • English, "K-Metric)
= Volume of gas sample passed through the critical orifice, corrected to standard conditions
TaN = Abso!ute ambient temperature (0R -English, °K-Metric)
K' = Average K' factor from CrUical Orif1ce Calibration
Vcrt:rld) Y=---= DGM calibration factor
.. V'ln(5,dl
AVERAGE dH@! =[ 1.525 I
2 dH@ = ( 0.75 9 ) dH (Vm(std))
V0,(std) Vm
Temperature Sensors
Reference In Out
OF
32
72
203
OF
33
73
202
OF
32
73
202
post 2013
I
' __ .. ,,~ ~ J.:.). r ~' -~ .. -----"--l....E_ -~ ' •.; --.....___:::. ~ --1
I
.. ~.-~..:______.....:.__•::
_::·.:-:} ~ i
~---Y
~ --... ·------B ._
} ~~~
) ... ·.Pili j t I H~--
=;----===~1.,...'~· ;?··::I··=··..::;'·-.-:::::::~.c.>­
,L ..... ~ ~~'1]~ _ L8
•. ..r-=, __ _
~:.·J.: l ~;:_:;,: :.: s
I :\I~
I( E.\'.\ r;:~
s~.~:~ ~; )JL \\An:~:
~ILIC(>\E r)!~
fl:_.~/~,c
.;_!':.._, ~_,_.-=4"'-Gt__.__,.v'-----·-
.;_:p,=--~~--ttJ:.· .:..J.,~(Ullfl--1
C~: ;..:;---1---
P: < y fJ,; 2..
r.: < 5~ P:= t..
z = ........;"_::():.....:::0:.__' _1-
-il I I
1[~3
1.01--
I
1'.'= -00 I
\\ = (p 'I'L
Z=
~1 ,;::; :·t:: :~:ur-:·
D<·,··<·c<:
i. ~ t
. Y ~ ~ <~n.o
I JO ~ ,
13~ !j '
11¢ £.., il \)
l [
l I
i~.
It:
, ..
L!o:.' \ ').. •
·'· 1 ,.
(~J
..... ) t'"· ..
,..-·-; r.t
~I
-·------., n· -
··-]·~-'·
I (
1: pc~ S l'itol ·1 ub~ lnsp~ction D3t~
P, =-
'.:.._' _· _4_4__:0:..--_ ...
rr.' • ' ,,, ~__:::."'t-__ _
n! ·~ :.;• "· ~ _.......::0=----
r.: <:S' fJ.~ _____ _
\\ .:. . 0 15"" tr)
\'c -' tr
z~ t;-:
. ·-=---. ·, ~ ~ ,• .'-::-', ~ ..., '.t.. "' --~ (.~--
TETCO
Sample Box TempGraLure Sensor Calibration
Date: 12/19/12 Calibrator· Mike McNamara Rcfacncc: Omega CLJ512A
Thermocou11le Temperature Temperatul'e Temp. Diff.
lJ nit ID Location Source Reference Sensor or Result
(Melli urn) ("F) ("F) ("F), P/F
Oven Water 33 34 I
Water 204 204 0
A Probe Out Water 33 34 I -
Water 204 204 ()
hnpingcr Out Water I 33
II
34
I
I
Water 204 204 0
Oven I
Water 33
II
35-
I
2
Water 204 204 0
B Probe Out Water 33 35 I 2
Water 204 204 0
lmpinger Out Water 33 34 1
Water 204 204 0
Oven Water 33 I :H I I
Water 204 204 0
c Probe Out Water 33 34 I
Water 204 204 0
1mpinger Out I Water 33 34 1
Water 204 204 0
Oven Water 33 33 0
Water 204 204 0
D Probe Out Water 33 33 0
Water 204 204 ()
Impinger Out Water 33 34 1
Water 204 203 -I
Oven Water 33 34 I
Water 204 204 ()
E Probe Out Water 33 34 I
Water 204 204 0
lmpingcr Ont Water 33 34 I
Water 204 202 -2
Oven Water 33 I 34 I I
Water 204 204 0
F Probe Out Water 33 34 I
Water 20 204 ()
Impinger Out Water 33 35 2
Water 204 202 -2
Jmpinger Out G I Water I JJ I 3tl I
I .. Water 204 202 -2 ll . ~-i I Water 33 I 35 2 lmpinger Out H Water 204 202 -2
I< Water 33 I 34 1
I).'.
lmpinger Out I Water 204 204 () ::
' Impinger Out J I
Water 33 I 34 1 -Water 204 203 ~I
·~ ~, 'I
.I
Water I 33 I 34 I ~ Irnpinger Out K Water 204 204 0
h·i -.,. ,;~
APPENDIXF
The testing followed the same procedures as outlined in previous protocols and tests at this
facility.
Prepared for:
Energy Fuels Resources
6425 S Hwy 91
Blanding, Utah 84511
Date of Report:
January 29, 2014
FOURTH QUARTER
RADIONUCLIDE EMISSIONS TEST
CONDUCTED AT
ENERGY FUELS RESOURCES
SOUTH YELLOW CAKE SCRUBBER
YELLOW CAKE DRYER BAGHOUSE
BLANDING, UTAH
December 16-17,2013
by:
TETCO
391 East 620 South
American Fork, UT 84003
Phone [phone]
Fax [phone] fax
CERTIFICATION OF REPORT INTEGRITY
Technical Emissions Testing Company (TETCO) certifies that this report represents the truth as
well as can be derived by the methods employed. Every effort was made to obtain accurate and
representative data and to comply with procedures set forth in the Federal Register.
Dean Kitchen
Revicwer: _____ _,;r;,fi?-==· -::.__ -'r.---1-i:..::-?t?..c:_"=-,-____..~~,--"'----__ _
Dat. : _____ _____:_/_-'--).....!....9_--f..~J __
~ DougOlsen
Reviewer:.~. ' \fu=--::.,______
Date: ___ _,__..>...:!oo<.-------'L-----'----------
ii
TABLE OF CONTENTS
Introduction
Test Purpose ......................................................................................................................... I
Test Location and Type of Process ...................................................................................... 1
Test Dates ............................................................................................................................. 1
Pollutants Tested and Methods Applied ............................................................................. .!
Test Participants .................................................................................................................... 2
Deviations from EPA Methods ............................................................................................ 2
Quality Assurance ............. , .................................................................................................. 2
Summary of Results
Emission Results .................................................................................................................. 3
Process Data ................................................................................................ "······················-3
Description of Collected Samples ........................................................................................ ·
Discussion of Errors or Irregularities .................................................................................. .3
Percent Isokinetics ............................................................................................................... 4
Source Operation
Process Control Devices Operation ..................................................................................... 5
Process Representativeness .................................................................................................. 5
Sampling and Analysis Procedures
Sampling Port Location ....................................................................................................... 6
Sampling Point Location ..................................................................................... _. ............... 6
Sampling Train Description ................................................................................................. 6
Sampling and Analytical Procedures ................................................................................... 7
Quality Assurance ................................................................................................................ 7
Appendices
A: Complete Results and Sample Calculations
B: Raw Field Data
C: Laboratory Data and Chain of Custody
D: Raw Production Data
E: Calibration Procedures and Results
F: Related Correspondence
iii
LIST OF TABLES
Table
I Measured Radionuclide Emissions ...................................................................................... 3
II Percent Isokinetics ............................................................................................................... 4
III Sampling Point Location ..................................................................................................... 6
IV Complete Results, South Yellow Cake Scrubber .............................................. Appendix A
V Complete Results, Yellow Cake Dryer Baghouse ............................................. Appendix A
LIST OF FIGURES
Figure
1 Facility Schematic Representation South Yellow Cake Scrubber ..................... Appendix D
2 Facility Schematic Representation Yellow Cake Dryer Baghouse .................... Appendix D
3 Schematic of Method 511 14 Sampling Train ..................................................... Appendix E
IV
INTRODUCTION
Test Purpose
This test project was conducted to determine the total radionuclide emissions from the South
Yell ow Cake Scrubber and the Yell ow Cake Dryer Baghouse exhausts in terms of Curies per dry
standard cubic foot (Ci/dsct).
These tests were for Th-230, U-Nat, Pb-210, and Ra-226.
Test Location and Type of Process
Energy Fuels Resources is located about 5 miles south of Blanding, Utah. Uranium ore is
processed into yellow cake, which is shipped to other facilities for additional processing. There
are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the
Yell ow Cake Dryer Baghouse. The packaging enclosure also discharges into the Yell ow Cake
Dryer Baghouse. The South Yellow Cake (SYC) dryer was the only operating dryer at the time
ofthe test. The North Yellow Cake dryer is currently not operational. The Grizzly Baghouse
serves as the main dust control device for the raw ore unloading and conveying to the processing
building.
Stack schematics are shown as Figures 1 and 2 in Appendix D.
Test Dates
The first test run on the SYC Scrubber was completed December 16, 2013 and the second run on
December 17, 2013.
One run was completed on the Yellow Cake Dryer Baghouse December 17, 2013.
Pollutants Tested and Methods Applied
The tests were a determination ofradionuclide emissions in accordance with EPA Method 5/114.
Test run filters and front wash residues were sent to Test America located in Richland,
Washington for radionuclide analysis.
Test Participants
Test Facility
State Agency
TETCO
Garrin Palmer
None
Doug Olsen
Jeff Graton
Deviations From EPA Methods
None.
Quality Assurance
Mike McNamara
Testing procedures and sample recovery techniques were according to those outlined in the
Federal Register and the Quality Assurance Handbook for Air Pollution Measurement Systems.
2
SUMMARY OF RESULTS
Emission Results
Table I presents the findings of the test in Curies per dry standard cubic foot. Tables IV-VI in
Appendix A have more detailed information.
Table I. Measured Radionuclide Emissions
South Yell ow Cake Scrubber Yell ow Cake Dryer Baghouse
Run# pCi/dscf pCi/hr pCi/dscf pCi/hr
1 7.65 5.966E +05 252.8 5.604E+07
2 7.55 5.950E+05
AVE 7.60 5.958E+05
Process Data
The process was operated according to standard procedures. All pertinent process data was
available for recording by agency personnel. Scrubber water flow, pressure drop readings (Llp)
were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (Llp)
were recorded and are found on the test run sheets. Production data will be submitted by Energy
Fuels Resources.
Description of Collected Samples
The test filters for the South Yell ow Cake Scrubber were moderately covered with a white or
pinkish white colored particulate. The front washes were clear in appearance.
The test filters for the Yellow Cake Dryer Baghouse were lightly colored with a tan colored
particulate. The front wash was clear in appearance.
Discussion of Errors or Irregularities
None
3
Percent Isokinetic Sampling
Each test run was isokinetic within the ±1 0% of 100% criterion specified in the Federal Register.
Isokinetic values for each test run are presented in Table II.
Table II. Percent Isokinetic Sam
Run#
2
South Yell ow Cake Yell ow Cake Dryer
Scrubber Baghouse
98
97
4
98
SOURCE OPERATION
Process Control Devices Operation
All process control devices were operated normally. Recorded scrubber water flow, pressure and
baghouse L1p readings were recorded and are found on the test run sheets or in Appendix D.
Process Representativeness
The facility was operated normally. Production data was retained by Energy Fuels Resources.
5
SAMPLING AND ANALYSIS PROCEDURES
Sampling Port Location
The inside diameter of the South Yellow Cake Scrubber stack is 12.75 inches. The two, four-inch
diameter sample port are located 28.24 diameters (30 feet) downstream from the last disturbance
and 6.59 diameters (7 feet) upstream from the next disturbance. Figure 1 in Appendix D is a
schematic of the stack.
The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch
diameter sample ports are located 28.38 diameters (454 inches) downstream from the last
disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port
locations are depicted in Figure 2 in Appendix D.
Sampling Point Location
Table III shows the distance of each sampling point from the inside wall according to EPA
Method 1. Each point is marked and identified with a wrapping of glass tape and numbered.
These points are determined by measuring the distance from the inside wall.
Table III. Sam lin Point Location
Sample Point
1
2
3
4
5
6
Sampling Train Description
Distance (inches) from Inside Wall
NYC Scrubber Dryer Baghouse
0.85
3.19
9.56
11.90
I I
0.70
2.34
4.74
11.26
13.66
15.30
To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-5/114
were followed.
All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent
interference of the sampled gas and particulate. The stack analyzers used to conduct Methods 1-
6
5/114 are constructed to meet the specifications outlined in the CFR. The temperature sensors are
K-type thermocouples. Heater, vacuum and pitot line connections have been designed to be
interchangeable with all units used by the tester. A 316 stainless steel probe liner was used for the
tests. Figure 4 in Appendix Eisa sketch of the Methods 5/114 sampling train.
Sample boxes were prepared for testing by following the prescribed procedures outlined in
Methods 5/114.
Sampling and Analytical Procedures
All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A,
Methods 5/114.
Quality Assurance
All equipment setup, sampling procedures, sample recovery and equipment calibrations were
carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance
Handbook for Air Pollution Measurement Systems.
7
APPENDIX
A: Complete Results and Sample Calculations
B: Raw Field Data
C: Laboratory Data and Chain of Custody
D: Raw Production Data
E: Calibration Procedures and Results
F: Related Correspondence
8
APPENDIX A
Table IV Complete Results, South Yellow Cake Scrubber
Table V Complete Results, Yellow Cake Dryer Baghouse
Nomenclature
Sample Equations
A
TABLE IV SYC Scrubber
COMPLETE RESULTS
ENERGY FUELS CORPORATION, BLANDING, UTAH
SOUTH YELLOWCAKE SCRUBBER EXHAUST
Symbol DescriEtion Dimensions Run #1 Run #2
Date 12/16/13 12/17/13
Filter# 6097 6098
Begin Time Test Began 9:30 11:21
End Time Test Ended 17:33 19:23
Pbm Meter Barometric Pressure In. Hg. Abs 24.75 24.80
Llli Orifice Pressure Drop In. H20 0.932 0.937
y Meter Calibration Y Factor dimension1ess 0.987 0.987
Vm Volume Gas Sampled--Meter Conditions cf 303.355 304.106
Tm Avg Meter Temperature OF 82.7 85.1
-IM' Sq Root Velocity Head Root ln. H20 0.5163 0.5197
W!wc Weight Water Collected Grams 261.5 257.4
Tt Duration of Test Minutes 480 480
cp Pitot Tube Coefficient Dimensionless 0.84 0.84
Dn Nozzle Diameter Inches 0.2530 0.2530
C02 Volume % Carbon Dioxide Percent 2.00 1.20
02 Volume% Oxygen Percent 16.60 17.80
N2 &CO Volume% Nitrogen and Carbon Monoxide Percent 81.40 81.00
Vmstd Volume Gas Sampled (Standard) dscf 241.634 241.655
Vw Volwne Water Vapor scf 12.330 12.136
Bws (measured) Fraction H20 in Stack Gas (Measured) Fraction 0.049 0.048
Bws (saturated) Fraction H20 in Stack Gas (Saturated) Fraction 0.087 0.083
Bws Fraction H~O in Stack Gas * Fraction 0.049 0.048
xd Fraction of Dry Gas Fraction 0.951 0.952
Md Molecular Wt. Dry Gas lbflbmol 28.98 28.90
Ms Molecular Wt, Stack Gas IMbmol 28.45 28.38
%1 Percent Isokinetic Percent 98.4 97.4 AVG
Ts Avg Stack Temperature OF 103.4 102.1 102.8
As Stack Cross Sectional Area Sq. Ft. 0.887 0.887
PG Stack Static Pressure !JLH20 -0.280 -0.280
PbP Sample Port Barometric Pressure In. Hg Abs 24.68 24.73
P, Stack Pressure In Hg. Abs 24.659 24.709
Q, Stack Gas Volumetric Flow Rate (Std) dscfin l.30E+03 1.31E+03 1.31E+03
Oa Stack Gas Volumetric Flow Rate (Actual) cfin 1. 77E+03 1.78E+03 l.77E+03
v, Velocity of Stack Gas :tpm l.99E+03 2.00E+03 2.00E+03
Curies Radionuclides per sample pCi 1849.0 1824.6
Crad Concentration ofRadionuclides pCi/dscf 7.652 7.550 7.601
ERrad Emission Rate of Radionuclides pCilhr 5.966E+05 5.950E+05 5.958E+05
* If the measured moisture content is greater than the saturated moisture level (supersaturated),
the saturated moisture value will be used in all calculations (40 CFR 60, Method 4, Section 12.1.7).
Symbol
Date
Filter#
Begin
End
Pbm
~H
y
Vm
Tm
'1/M
W!wc
T,
cp
Dn
C02
02
N 2 &CO
Vmstd
Vw
Bw.
xd
Md
M.
%1
Ts
A.
Po
PbP
Ps
Q.
Qa
Y s
Curies
Crad
ERr ad
TABLE V
COMPLETE RESULTS, PM
ENERGY FUELS CORPORATION, BLANDING, UTAH
YELLOW CAKE DRYER BAGHOUSE
DescriEtion Dimensions Run#1
Date 12/17/13
6099
Time Test Began 14:06
Time Test Ended 16:10
Meter Barometric Pressme In Hg. Abs 24.80
Orifice Pressure Drop ln. H20 1.967
Meter Calibration Y Factor dimensionless 0.988
Volume Gas Sampled--Meter Conditions cf 105.944
Avg Meter Temperature OF 85.5
Sq Root Velocity Head Root In H20 0.8818
Weight Water Collected Grams 17.3
Duration of Test Minutes 120
Pitot Tube Coefficient Dimensionless 0.84
Nozzle Diameter Inches 0.2235
Volume % Carbon Dioxide Percent 0.00
Volwne% Oxygen Percent 20.90
Volume% Nitrogen and Carbon Monoxide Percent 79.10
Volume Gas Sampled (Standard) dscf 84.467
Volume Water Vapor scf 0.816
Fraction H20 in Stack Gas Fraction 0.010
Fraction ofDry Gas Fraction 0.990
Molecular Wt Dry Gas lbllbmol 28.84
Molecular Wt. Stack Gas lbllbmol 28.73
Percent lsokinetic Percent 97.6
Avg Stack Temperature 'F 80.8
Stack Cross Sectional Area Sq Ft. 1.396
Stack Static Pressure In H20 -0.73
Sample Port Bmometric Pressme ln. Hg. Abs 24.73
Stack Pressure In Hg Abs 24.676
Stack Gas Volumetric Flow Rate (Std) dscfin 3.69E+03
Stack Gas Volumetric Flow Rate (Actual) cfin 4.63E+03
Velocity of Stack Gas tpm 3.32E+03
Radionuclides per santple pCi 21353.2
Concentration of Radionuclides pCi/dscf 252.7982
Emission Rate ofRadionuclides pCilhr 5.604E+07
Dryer Bag house
General Nomenclature
%1 = percent isokinetic, percent
A.=(D.2 /4)•n
AS~P = see "~p
Btu = unit heat value (British thermal unit)
Bw.; = fraction of water in stack gas (may have designation of "measured" or "saturated")
"measured" represents measured moisture based upon sample volume and water collected
"saturated" is a calculated value based upon stack pressure and temperature
C0 = average of initial and final system zero gas calibration bias checks (ppm, percent)
Cavg = average gas concentration (as measured)
C8 = concentration of particulate matter, back half (gr/dscf,Ib/dscf, etc.)
Ccond = concentration of condensibles (grain/dscf)
Ccors = concentration of coarse particulate (gr/dscf)
Coir = measured concentration of a calibration gas when introduced in direct calibration mode
Cr.= concentration of particulate matter, front half, actual stack flow (gr /act)
CF = concentration of particulate matter, front half (gr/dscf,lb/dscf, etc.)
Cgas = Cavg corrected for initial and final system bias checks (Equation 7E-5)
Cm = average of initial and final system upscale gas calibration bias checks (ppm, percent)
Cma = actual concentration of upscale calibration gas
Cmetal = concentration of metals (ppm, ~g/fe, etc.) atomic symbol replaces "metal"
C02 = percent carbon dioxide in the stack gas
cp = pitot tube coefficient (0.84)
CPMIO = concentration ofPM10 particulate (gr/dscf)
c,.d =concentration ofradionuclides (pCi/dscf)
CS = measured concentration of a calibration gas when introduced in system calibration mode
Cx = Any species symbol may replace X. Units may be expressed as ppm, lb/dscf, etc.
Cx (carr)= actual gas concentration corrected to required percent 0 2
Curies= Measured radionuclides per sample. Units may be pCi or uCi.
De= jet diameter (em)
D/F = Dioxins and Furans (See laboratory report for D/F descriptions and nomenclacture)
~H = orifice pressure drop (inches H20)
~H@ = orifice pressure (inches H20)
~d = orifice pressure head (inches H20) needed for impactor flow rate
Dn = nozzle diameter (inches)
~p = stack flow pressure differential (inches H20)
Dp50 = 50% effective cutoff diameter of particle (em)
D.= diameter of the stack (feet)
EA = percent excess air
ER8 = emission rate of back half particulate (lb/hr)
ERcond = emission rate of condensibles (lb/hr)
ERcors = emission rate of coarse particulate (lb/hr)
ERF = emission rate offront half particulate (lb/hr)
ERgas = emission rate of a gas (lb/hr)
ERmmBtu = emission rate per mmBtu of fuel
ERPMIO = emission rate ofPM10 particulate (lb/hr)
ER,ad =emission rate ofradionuclides (pCi/hr)
ERx = emission rate of compound which replaces X. Units are usually in lb/hr.
F0 = Dry based fuel factor. Ratio of the gas volume of the products of combustion to the heat content
See 40 CFR 60, Appendix A, Method 19, Table 19-2 for fuel factor values.
K, = Cunningham slip correction factor
A,= mean free path of molecules in gas phase (em)
mmBtu = million Btu
General Nomenclature
Mcond = mass of condensibles (milligrams)
Mears= mass of coarse particulate (milligrams)
Md = molecular weight of stack gas, dry basis (lb/lb-mol)
MF = mass of particulate on filter (mg)
MFP = mass of particulate matter on filter and probe (mg)
mmBtu = million Btu
Mp = mass of particulate matter in probe and front wash (mg)
MPMJO = mass ofPM10 particulate (milligrams)
M,. = molecular weight of stack gas, wet basis (lb/lbmol)
Mx = mass of species "X". Units may vary and other descriptive subscripts may apply.
lls = gas viscosity (poise)
Mwx = molecular weight of gas species (g/gmol)
N = number of jets per plate
N2 = percent nitrogen in the stack gas
0 2 = percent oxygen in the stack gas
..Jill'= average of the square roots of M' (may also be referred to as ASM'}
.../M'1 = square root of M' at point 1 of the current test, Method 201A
.../t'lP1' = square root of t'lP at point 1 of the previous traverse, Method 201A
.../t'lP'ave = average of the square roots of M' from the previous traverse, Method 201A
Pbm = absolute barometric pressure at the dry gas meter (inches Hg)
PbP = absolute barometric pressure at the sample location (inches Hg)
P0 = stack static pressure (inches H20)
P5 = absolute stack pressure (inches Hg)
Pstd = absolute pressure at standard conditions (29.92 inches Hg.)
e = time of test (minutes)
81 = sample time (duration in minutes) at first sample point for Method 201A
Sn = sample time (duration in minutes) at sample point "n" for Method 201A
81est~ target test time for Method 20IA (minutes)
Q. = stack gas volumetric flow rate (acfm)
Q5 = stack gas volumetric flow rate (dscfm)
Q50 = actual gas flow rate through the cyclone (acfm)
Qsce = actual gas flow rate through the impactor (acfm)
Qw = wet stack gas std. volumetric flow (fe/min, wscfm)
R = gas constant (21.85 inches Hg*fe/(lbmol*R))
Pp = particle density (I g/cm3)
Ps = stack gas density (g/cm3)
T m = stack temperature (°F)
T5 = stack temperature (°F)
T51d = absolute temperature at standard conditions (528°R)
Tt = Duration of test run in minutes. Also see 8
urn= mean molecular speed (cm/s)
Vm = sample volume (fe) at meter conditions
Vmstd = volume standard (dscf), sample volume adjusted to 68°F and 29.92 inches Hg.
V5 = velocity of stack gas (fpm)
V w = volume water vapor (set) at 68°F and 29.92 inches Hg.
Wfwc = weight of the condensed water collected (grams)
~ = fraction of dry gas
Y = meter calibration Y-factor (dimensionless)
\If = dimensionless inertial impaction parameter, 0.14
General Sample Equations
%1 = Vmstd • (Ts + 460) • 1039 I (8 • Ys • P5 • Xd • Dn2)
As = (D/ I 4) • 1t
Bws = V w I (Vmstd +V w)
Ca = M8 • 0.01543 I Vmstd
Ccond = Mcond • 0.01543 I Vmstd
Ccors = Mears • 0.01543 I Vmstd
Cra = Tstd • Crp • Ps • Xd I [Pstd • (Trn + 460)]
Cf= Mrp • 0.01543 I Vmstd
CPM10 = MPMIO • 0.01543 I Vmstd
Crad = CuriesiVmstd
Cgas (carr)= Cgas • (20.9 -desired %02) I (20.9 -actual %02)
case DPso = ...J [J..lS • \jf • N • 1t • D/ • 18 I (Kc • Pp • Qsce • 4)]
0.2091 0.7091 PMro DPso = 0.15625 • [(T5 + 460) I (Ms • P5)] • (lls I Q5c)
ER:ond = Ccond • Qs • 0.00857
ER:ors = Ccors • Qs • 0.00857
ERF = Cf • Qs • 0.00857
6 ERgas = Pstd • Q5 • Mwgas • Cgas • 60 I (R • Tstd • 10 )
ERgas = Cgas(lb/dsct) • Qs • 60
(Either ERgas equation gives equivalent lblhr values to 3 sig. figures)
ERrnrnBtu = Cgas(lb/dsct) • F d • (20.91(20.9 -%02), Method 19 Equation 19-1
ERPM10 = CPMIO • Qs • 0.00857
ERrad = Crad • Qs • 60
Kc = 1 + 2 • A • 1.257 I Dp50
A= 1-ls I (0.499 • Ps • Urn)
Md = C02 • 0.44 + 0 2 • 0.32 + N2 •0.28
Ms = (Md • Xd) + (18 • Bws)
1-ls = [51.05 + 0.207 • {Ts + 460) + 3.24 ·10-5 • {Ts + 460)2 + 0.53147 • %02 -74.143 • Bws] • 10-6
Ps = Pbp + (PG I 13.6)
81 = (...JAP1' I ...JAP'ave) • (81est I pts)
en= 81 • ...JAPn I ...JAP1
Qa = Ys • As
Q5 = Qa • Xd • Ps • Tstd I [(Ts + 460) • Pstd]
Qsc = [(Ts + 460) • Pstd I (Tstd • Ps)J • [(Vmstd + Yw) I 8]
Qsce = [(T5 + 460) • Pstd I (Tstd • P5)] • [(Vmstd + Yw) I 8]
Qw= QsiXd
Ps = P5 • Ms • 3386.39 • 10-6 I [R • (T5 + 460) I 1.8]
Um = 100 • ...J {[R • (T5 + 460) I 1.8 • 8 • 103] I [1t • M5]}
Vmstd = Vm • Y • Tstd • (Pbrn + AH I 13.6) I [Pstd • (Trn + 460)]
V5 = 85.49 • 60 • Cp • ...JAP • ...J [(Ts + 460) I (Ps • Ms)J
Yw= Wtwc • 0.04715
Xd = 1-Bws
APPENDIXB
South Yell ow Cake Scrubber
Preliminary Velocity Traverse and Sampling Point Location Data
Particulate Field Data
Yell ow Cake Dryer Baghouse
Preliminary Velocity Traverse and Sampling Point Location Data
Particulate Field Data
B
South Yell ow Cake Dryer Scrubber
Preliminary S Y Cake Serb
r
Facility Energy Fuels
Stack Identification South Yell ow Cake Dryer Scrubber
lA Date tz!r.. .~J~
N Barometric Pressure
Pbm Z. Y· J-5fn Hg Pbp ·2 v/-6-Y" in Hg
B ---+ I Static Pressure (P0) l:"ltiis-in H20 • oz.~
Estimated Moisture (Bw.) 4-6 % -Sample Height from Ground 70 feet
Comments:
Stack Dia. 12.75" Reference: 0"
Ports are 7' Upstream from next disturhancc
Ports arc 30' Downstream from last disturbance
Traverse Percent Distance From: Ports
Point Diameter ID Reference A B c D E F
1 6.7 0.85 0.85 .,.,
·1 L ..... .1-/()
2 25.0 3.19 3.19 /OU , $) ,.~ . .,..,
3 75.0 9.56 9.56 1oo. JSi' ,..,
• "1'...-l
4 93.3 11.90 11.90 ~r . ~t-'S' • 3<ll
Averages:
Ts L Flow --------
.'\P ..J.'\P --------
KEY=>! ~T_s __ ~.'\~P~L-F-lo_w~~
f"'1 ~ Field Data Sheet
Plant: Ener~ Fuels.,
Date: \ ) ( ep /1 ---s
Traverse Time DGM L\P ~H (inH:O) Vacuum
Pomt
1
1
1
2
2
2 .
3
3
3
4.
4
~
1
1
1
2
2
2
3
3
3
4
4
4
Total
Average
Clock Min (9)
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Location Souttftellow Cake Dryer Scrubber
Operator: ~
Temperatures !"fl
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';;01-D
tZ-1-
. DGM before Leak Check Vac ("Hg) Rate (ft31min) DGM After Leak Check Vac ("Hg)
\ f I Run#_ Page_o--J
~
A r Bo N
Stack Diameter 12.75" Poll Reference ____,Oc.." __ _
Ports are
Portsar'
_7_' __ Upstream from next disturbance
30' Downstream from las\ dilnurb:lril:C:
Assumed Moisture
Probe 7 -:f. G
Nozzle Calibratiori
4·6%
Cp___QM
. Z..<>"') . ~5"2 ·Z>) . 2 >3
Avg D. · Z 5} inches
Gas Bag (... -o ""'+
Console ~
Y-Factor ~ {'}-
L\H@ (. (, 2.Uin H20
Barometric Pressures
Pbm Z'f-1s-in Hg
Pbp "2.. 'f '(p 8" inHg
Po --c z ~J in H20
Leak Check ~
ilJ/min {)_-oD:j
vac 10 Hg -z..z.....
P1totRate~
InH,O 5..:....L
~
o · C2"' -:j-
~~
Q.;...Q ss:
Water Collected 2. (, f · .5-
TimeSampled ~
Review ~
I
K= @Tm
K= @T.,
g
min
Rate (te/min)
(1/'-c; Field D"ta Sheet
Plant: Energy Fu~ls
Date 10/1-;} V)
'"'~-)YTCO C.
Filter fp ~ Sample Box____l=::__
Location: So~Yellow Cake Dryer Scrubber , I
Operator· i1 ..1. .q v~
Trnverse Time DGM 1.\P .'~H "nH,Oi \-.><....m Temperatures ,.,, DGM 'fcmp tT,.J.
Pomt Clock Min (8) ··~"· •htll 0 Desired Actual •• ,.. Stack (T,) Probe Probe out Oven Effiuent Out In
Page J o( L Run# Z
r Bo N
0=Ru:z J o 92.olf~ -~CI _qt, .q~ v /Ou ~)D 11s-;q z'-((p 5 !.f ';-L.r S.7
1 '--0 /0'-{. t 5; 7 ---~ ' I . o; /·l>' l---J l)L-/ ~-;.;----7 50. 1.. (;; D ~ \ ft, D &--~!Stack Diameter 12.75" Port Reference __,0'-"---
1 1./0 tf-:}'?,b-'-L J~! 1-c< 1-D$ /1/ lo4 1.~'1 'le;-1' zl:.._o 5(j --:;.1.---~h
2 II I (;o 11 1~.--{-{,5 ll~~t.ll f·o~ I {-o'1ll'7.-II 1-o-t ' ~.~S~l,.~l?b1-:IU'1 11:71-I 'qo
zo 2
~0 2
~ ~3~1~--~--4~~~~~~=-~~~~--~~~~~~~~~~~~~~~~~~--~~ ~~ 3
~~ 3
~ --4~1~--fU~4~~~~~~~4~~~~~~~~~-~~~~~~~~pL~~~~~~
zo ~4~~--~~~~~~~~~~~~~~~~~~~~~~~~4+~~~~~~~~~
l.{/7 4
'{ 1\-'1 l tc;:z.-~1 z-<t1Jiz.'1~ .fPov li-J_s--11 ·f:r l.v-1-'J 'v-II wGflz_s-01 1.. ?sl -z-(.(~1 uvll s 'i I ~ G
1.0 1 -z. fllon -c__.~-~~'> II ~Zr-1 II -~if T~lv IIJ Q)_I_Z---1~ I t---z,t:J 1.c;-1 l 't1 lll fiLII ·q ¥'
'iO 1 'Z. -?0 11 ~-f).j \\ lr.:t:t=II-S(<-{ I • ~v/_ll,z_:--11 ! D¢" I "Z--Lj~J, ~~ I 'l-)~ lf1l["F~J &'c.-,
~ 2 l3(>o ll_l~S' ~71]~ t) IC~.S£1---11 V lt7v-t:" l;;_f:tf11-~lt?,1-6 '1 4 C IC$""J?l~fi.S
zo 2 --L3zoJ Z.ez1 .uiiJI-~tpJ! .:c,r T-Pill l ~ ll..liD_It/{0 _L1_1flll_Cf'VI :U[J!i-:Ll_¢s
~0 2 ;,L:tt'II~Dl:j·J~fp~-&7fll ,C/J .. -LJ.C\-~1 ll~ljgC/1 rf"'tz.:rz::roJl>it1l 'Zh llt60t I ~~
Ports are 7' Upstream from next disturbance
lPons are 30' Downstream from last disturbance
Assumed Moisture &
Probe L T 4-6%
Cp 0.84
Nozzle Calibration
. .LB._ ~ . Z-7') . zss
Avg D., • 't ~-) inches 1
Gas Bag {__ -0 I
Consok &
Y-Factor • ~ y F
L.\H@ UW1H20
Barom~tric Pressures
Le>k Chet:k
t.-1 ...,_() Pb"' l. ~ . :iiT m Hg
Pbp '2. '"t • 1= 5 in Hg
J>C" (C). z_ ~ )in H20
\,. ?·
Pre Post 1 (p -3 3ro lb_-z:Z~?'~~11·1!2."1[~:1-J-·Y!'LJC2~1 ~~~ _I'Z>it:tJ ~-zL{..:u q72J[¥<f I 5~ rlllmin ~y 6---:ool"
2..z_ ____L2 7-" _3
..;.o 3 l-4 zo 4
<{U 4
Total
Average
[3::~::~::r=i,~-'111JLjdJEi'IJ, y''f,ICZJC:u I UMil:ti5IZd~J3_j_IUftl -~ s:
4oo ii.-1.J1:-f7_.:~ll-1=rll-){1 T--=-~]!-/_]~-1·7.&~:1:1_~<-\ ~ ~CJII ~1--1~
c.uo II ,f,~q\c;~ll -1_c;-.l4-TI. ~ 1-lL '7 11 ct Sf I i ~~_l_'l 7~1-z~<)l (2}~'1'11<6<?'" I q r ~
~t¥n5~l -tq ~~·~t=l ·~t-jCTIF!q ~~1iCtt-5~=f.<:'{J1f~~· ~~~~ gf ~~ ?'if~'J -tC(' -v ·¥.f l~~b1..<.t1Z -;'1 i'-lTi; ~
_!_1;~ jl-\ ~t7Jr31~W._.--T---, ---II -~---..---.-v--~ -r 'r .-----.
'JOY-fow ~ tZ>t.(-47 1 t.t-q'1
-J -s\'t1 -'1~1--
1.:-\5 \
toz...\
DGM before Leak Check Rate (te/min) DGM After Leak Check
Lfos-t
G5 · I
vac in Hg
Pnor R<~te Q . Q
lnH,O ~
o.D
q .2
Water Collected 7f7• ':/ I!
Time Sampled ~~ mm
Review ~
K=
K=
1i;Tm
o:~~T II
Yell ow Cake Dryer Baghouse
Prelim 6 pts blank
Facility Denison Mines
Stack Identification North Yell ow Cake Drver Baghouse
Date
r Barometric Pressure
8 Pbm in Hg Pbr in Hg
N 0 Static Pressure (P G) in H20
A Estimated Moisture (Bw,) I %
Sample Height from Ground feet
Comments:
Stack Dia 16 Reference: 0
Ports arc 57" Upstream from next disturbance
Ports are 468'' Downstream !Tom last disturbance
Traverse Percent Distance From: Ports
Point Diameter ID Reference A B c D E F
1 4.4 0.70 0.70
2 14.6 2.34 2.34
3 29.6 4.74 4.74
4 70.4 11 .26 11.26
5 85.4 13.66 13.66
6 95.6 15.30 15.30
·.
Averages:
Ts LF!ow ---------
~P __ _ ..J~p ----
KEY=> ~p LFiowl
Ll:i Fteld Data Sheet
Plant: Denison Mines
Date: D~c. I}! ].O(b
TETCO
Filter_~_:r}___ Sample Box __ E __
Location: YellowcakcDryOt Baghousc
Operator: raul L K ·k l-.en
Trav~rse Time DGM t.P .1H (mH20) Vacuum Temperatures ("F)
Potnr Clock Min(S) ,rr'~ {inH10) Desired Actual (mil~) Stack (TJ Probe Probe Oul Filter Eft1uent
,~ 1 t'i:oh 0 '1~1--~~ (... ,:ft) i-1'3 1-U -;.a 8v 2.-rZ-. ).ipi_p 2(,{~ §'I
2 !;:) '-{i-5, 'fD[p ,t--v \.18 \ _1£ 3.0 3v 2(._tz, 2.:;?-;z..:,-(>:1 lf9
3 'Z..o 4Jt <f ' ' ':.<? .'13 2.-30 z..3C l!i.D ~-z._ J_l-{~ 253 2S~ so
4 :y 3o '-H.'{3.~ . czg .2,_-'-1"2, ~-(.,12 '-f,Z) 9Z.. ,;L7z_ 2$'Z.. z:;z, c., l -I
5 '-to ?o:>.>.-rre ,'fs 'j_,Cf'l 2·'-f"Z-Lf. 0 -D r ).'{~ }..3lf 2-7§" :;z..
6 .:,o 5t3.S~1-. 'i3 '2._.30 2 -3o '-{.o '3 1 .2~&> 2)'-f z~q S!
}!, 1 1~:10 &o ~23-'-~ ·"~ f,LfO /-'--lC 3 •() ISO 2-f,Z--2<-tl 2.'-fD '16 -
2 'fc '7?0 -~ctg • t-1.(;, I.(<;' I. 15" '3 .o 20 :l~L{_ "JG/.D )110 tr.6
3 ~D s~ t.~?3 .. ~i 7, ;,as-/,05 3-0 eo )c.. I ).<{0 2 .... l!l £.j{'
4 '1-o S'-1'1. 6fl.{ {,oo .l.-'1~ .,(, LJ'1 tJ.o '2>0 2..$'0 )..__;$" 2 "}$"' '-t~
5 /00 5 5'i.'3~9 ,q~ .2. 31--2-3:f--<i.o \?0 ?..-"-t'f ;}.-<{(., )4~ '-/(~
6 11-0 6 (; '{ lZ-0 .$"B J..fq 2-l!f .l.f-v Bo ;1_'-j/ ,Nt'.Y J-'1) <-t&:>
it?; tO rt.---0 ~73, <;_~
~ ---
Total lOS. U(../_Lf j" {0, S8t'l,. 1~.vv 41-D
/
.......... !::! ... --
Time Baghouse6P S"aghouse6P >I' 5/l..)-clrrwf\ Comments Time s~4(J vf I'!~ r:;{ S,O tS'' 12.. iO.o
1'-i',l-~ q,8 t5' [.1· 10.()
I"-\ :;'3 !D .o tS ·'-114 'L)
! 11:56. IO·o t ):~ "' ~--? "b D ,,n'' 'J -. ~ . '". ..,\
DGM 'rcm~(T.)
Out In
J? i-f rZ--::;r.;
4 t -:;y [?-{
?-& 13
1-ti 7P
8D loo
~I' tt8
$12.-'?!(
~2.-yq
'I$ "e..-'tB_
<(t /00
t-~" l;o c)
Page_l_o( _ __L Run# __ 1
i B Ao N
St~ck·Diameter 16" __ Port Reference _0.0"_
Pons are
''l'otts ~rc
~Upstream from next dtsturbance
468" Dl:!wnm=n f'Wmll$1 di.slurh .. ~cl:.
Assumed Moisture
Probe 18 Cr
_ _:_ __ %
Cp 0.84
Nozzle Calibration
, zz.~ . 2--z '3 "z:zA . -zz.t/
Avg o., 2!.->5" inches
Gas Bag Ambient Air
Con.soJe_l
Y-Factor ' 'f8fJ
t.H@ )J~8Z-inH20
Barometric Pressures
Pb '-'-1-f!D in H" Pb~ :1-'i -f} in H;
P--. r'!J m H,O
Le>k C'b•ck Pre ~
ti3/min O.co<j ~:
vac.i11Hg z..(_.o <.,..o
Pnot Rate o.ov D-OQ
InH,O q.~ Gj,S
·""'~? l • Water Collected t T' S
Time Sampled 1 2 0 min
Review P R. \(..
]._o? ':J
K= ·~Tm
-'" .=;x:•a
I _;....--j), (("~{ OL{Jt>--' ''f'l/{7 J I /1 l , , ....
il-!~!.~8
?n,t-t/h%(
-,
South Yell ow Cake Scrubber
Sample Recovery
Gas Analysis Data (ORSA T)
Yell ow Cake Dryer Baghouse
Sample Recovery
Gas Analysis Data (Ambient)
Chain of Custody
Lab Analysis
APPENDIX C
c
South Yell ow Cake Dryer Scrubber
METHODS
Facility: Energy Fuels
Stack Identification: SYC Scrubber ~~~~~---------------------------
IMPINGERS
Run: Sample Box:
lmpingcr Number
2 I 3 I 4 I 5 ~11-T'U~-N\ll'l">l\f:.R..
!mtia! nlumc ofliquid (H20) in impingcrs, (ml)
JMPINGERS
Run : Sample Box:
lmltgcr Number I 3 I 4 I' 5
Initial VolunJc of I iquid (H20) in impingers, (ml)
Net (g)
Total (g)
IM£1NGERS
Run: Sample Box:
)mpingcr Number
I 2 I .1... I 4 I 5 -lultln.l Volume of liquid (H20) in impingers, (ml)
drop out 100 I arop out I 100 I
'
Final (g)
I
Initial (g)
Net (g)
Total (g)
IMPINGERS
Run: Sample Box:
L 2
lm£1gcr· Number
5 -I 3. I ...!. I
lnithtl Vv!umc of liquid (H20) in impingers, (ml)
drop out 100 I drop out I 100 I
' '
Final (g)
Initial (g)
Net (g)
Total (g)
LfT ·1 ======
Date:
6
6
Silica Gel
6 -
Silica Gel
"
..L
Silica Gel
,-
p ]ant M Q<r-, ""' (
Analytical Method. __ ~='-:....:....--
Date 1 z,L t-
Test No.~
Gas Bag No. -(---()~-::;:,}r-
Ambient Temp--#---
Operator~
Dote~'5
TestNo. L ,
Gas Bag No. C -{...' f
Ambient Temp '711
Operator ~i(\
Date -----Test No. -----GasBagNo. -----Ambient Temp ____ _
Ope.rator ____ _
Gas
C02
0 2 (Net is Actual 0 2
Reading Minus Actual
C02 Reading).
N2 (Net is 100 Minus
Actual 0 2 Reading).
Gas
C02
0 2 (Net is Actual 0 2
Reading Minus Actual
C02 Reading).
N2 (Net is 100 Minus
Actual 0 2 Reading).
Ga~·
C02
0 2 (Net is Actual 0 2
Reading Minus Actual
C02 Reading).
N2 (Net is 100 Minus
Actual 0 2 Reading).
I
Actual
Reading
z.o
If-~
"' ·:_~1~
I
Actual
Reading
(·1.__
(l·O
I ~ I '
.,
~ \t;i
I
Actual
Reading
t~' ,,~ 'j:.~~ .... ~
Location. __ S_,.....:::.C,::_ ____________ _
RUN
2 3 Average
Net Actual Net Actual Nd Net
Reading lteadinr, Volume
Z·c:> 2·.c.,.~ 2-c.J 2-o z.o 2.6
lt..-C, t&--h /~(/# ~f--~ t~fd I '-·b
' . -.. !
,. ~.=i:~t. )ll.i ;;;;~rl-b. ,.
RUN
2 3 Average
N~t Actual Net AcluRl Net Net
Reading Reading Volume
I •L 1' c \.z: I . z.: \ .z I· Z~
I ~ . ~, 1'.:..t.u ( :1.(.-lc;(• 0 ·-, I -~1 -~
' i) I r ·~ ' J
I ~~--.. ..
j;, :~1-~~> ;~··
RUN
2 3 Average
Net A dual Net Actual Net Net
Reading Reading Volume
~.~:·! '
~I4,'''
0 I -~· ~
CO is not mc.asurcd, as it ha~ the same molecular weight as N2
Yell ow Cake Dryer Baghouse
Method 5
Facility: Energy Fuels Date:
Stack Identification: Yellow cake Baghouse
IMPINGEI!S
Run: Sample Box:
Fiho r Number lmpmgcr Number
.L 2 I 3 I 4 I s 6 -lnilial Volume of ll<tllld 1110) in hnptngcrs. (ml)
IQO
JMPINGERS
Run: Sample Box:
Filter Number
2 ! ~ I _1_ I s
_Initial Volume of liquid (Hp) in impingcrs, (ml)
100 100 I I SilicaGel I
Final (g) --------r-------+-------+-------+-------1--------
Initial (g) --------~------+-------+-------1-------1------
Net (g)====b::===b===:!:::::==="'====::::!::::===
Total (g) ======
IMP!NGERS
Run: Sample Box:
Filter Number lmpmger Number
..t. I I ....L I ...1. 6
lnilial Voh.unc o. llquid(II.JO) in lmpingcrs. tml)
100 100 I I SilicaGcl I
Final (g) ------+--------1-------+--------+--------1-------
Initial (g) _______ +-------+------+-------1--------+-----
Net (g)====b===:!:::::===='====::::!::::========
Total (g) ======
Chain of
Custody Record
TAIJ4124(10G7)
Client
Tetco
,1rkircss · 391 East 620 South
Cily American Fork I Stale I Zio Coda
~ Ut 84003
Proiect Narnil:snrJ w..aliOtl fSrei.liJ
Energy Fuels 2013 4th Quarter
Ccn~racVPvt~>tUS O:ltoriQuo~ No_
Sample 1.0. No. and Description !
(Contains~ for each sample may be combined on one line) Dale
R1 Dryer BH filter {6099) and beaker 12/17/13
R1 SYC Scrubber filter (6097) and beaker 12/16/13
R2 SYC Scrubber filter r609Bi and beaker 12/17/13
Temperature on Receipt __ _ Test America
Drinking Water? Yes 0 NoD THE LEADER IN ENVIRONMENTAL TESTING
Fw/OOMll~
Dean Kitchen
Tc~~l>/urnbar (;.tell C«kl)IF~~x Nurnbor
801-492-9106
Site Contacl J Lab Contact
Sc:ott Cluisl~nsen, G1rr1tn Pelmer
Clfrrief/VV<tybi# Number
Matrix
10:00
11:00
Containers &
PreseNatives
~,@,8 ~ ~ ~ -<; ...,o -lb"' ~I ~~~
I I
~ 0 :!3 ::J ~ ..:, ± "' ,_ ::> a:
X X X
X X X
X X X
Date
12/18/2013
Lab Number
Analysis (A !taGh list If
more space is tl68ded)
ol I I I I .... N -a "' .. _,1 I I I I
X 1 I I I I
I i X
X ,~,~ I
I·
1 I I I
I
I
I
I
Ci'Jlin-or CUsiOdv ~umbi>r
Page of~~~
Special Instructions/
I I Conditions of Receipt
PoiSibJe H~tZB!d laen/illr:atian $llfl'IRI~ 00~ (A fee may be a9Sesssd if sumples are mtainod 0 Non·Hazsrrf 0 F/smmablo 0 Skin Irritant 0 Poison El 0 Unknown 0 Rotum To Client
TIJ!tl A!Ourtd Time Rl1qtlffY.I
0 0/spcsal By Lab 0 Archive For ___ Montl!s l<>ng9r tflan 1 month)
QC RtiqufremiiJ!$ (Sp&:Hy)
0 24 Hours 0 48 Hours 0 7 Days 0 14 Days 0 21 Days 0 Other as ll.er method
I.P.f1/l~r:11~ CL LI -loa. !$· IT-. .J'· Rsce;~fl(/ ay -~--I.OQ.to I Ttmo 1 2./i<J!r~ 12.: 00~ ~
o>. «cJI~u!>hed SjH _("'cr-I rrm~ ·ro~ec:elv6d8y -I Dlii!T I nm ..
3. R~'iflqui!Jillld By j fllfM J Tftrnt' r-Recervad-Sy (.Ota
1
-/vng
~nts
When Complete Email to: Dean or Paul [e-mail]
DISTRIBUTiON: WHiTE -Rerurrred ro Clf!!lllw(rn Flepf;r.; t;:W'J.ytl' -S!Irys •i•iin'"lttlo::"S"'IIl=rripi(l;o::· :;;::-, "PI"'N."''K'·-,n"'~:;:lri;;;. ec;p=y:-::------------------------------------
~-
SDGNo. Order No.
47656
TestAmerlca Inc
t•ptSTLRchTitle v3.73
TestAmerica Laboratories, Inc.
Analytical Data Package Prepared For
Denison Mines (USA) Corp.
Energy Fuels 2013 4th Quarter
Radiochemical Analysis By
TestAmerica Inc
2800 G. W. Way, Richland Wa, 99354, (509)-375-3131.
Assigned Laboratory Code:
Data Package Contains 18 Pages
Report No.: 58563
Results in this report relate only to the sample(s) analyzed.
Client Sample ID (List Order) Lot-Sa No. Work Order Report DB ID
R1 Dryer BH filter(6099) J3L300411-1 M2QVR1AE 9M2QVR10
and b
R1 Dryer BH fllter(6099) J3L300411-1 M2QVR2AA 9M2QVR20
and b
R1 Dryer BH filter(6099} J3L300411-1 M2QVR1AC 9M2QVR10
and b
R1 Dryer BH fllter(6099) J3L300411-1 M2QVR1AD 9M2QVR10
and b
R1 SYC Scrubber J3L300411-2 M2QVT1AE 9M2QVT10
filter(6097) a
R1 SYC Scrubber J3L300411-2 M2QVT1AA 9M2QVT10
fllter(6097) a
R1 SYC Scrubber J3L300411-2 M2QVT1AC 9M2QVT10
filter(6097) a
R1 SYC Scrubber J3L300411-2 M2QVT1AD 9M2QVT10
filter(6097) a
R2 SYC Scrubber J3L300411-3 M2QW1AE 9M.2QW10
filter(6098) a
R2 SYC Scrubber J3L300411-3 M2QW1AA 9M2QVV10
filter(6098) a
R2 SYC Scrubber J3L300411-3 M2QW1AC 9M2QW10
filter(6098) a
R2 SYC Scrubber J3L300411-3 M2QW1AD 9M2QW10
filter(6098) a
Batch No.
4002022
4002023
4002024
4002025
4002022
4002023
4002024
4002025
4002022
4002023
4002024
4002025
Test America
THE LEADER IN ENVIRONMENTAL TESTING
January 28,2014
Denison Mines (USA) Corp
1050 17th Street, Suite 950
Denver, CO 80265
Attention: Dean Kitchen
Date Received at Lab
Project Name
Sample Type
SDGNumber
I. Introduction
Certificate of Analysis
December 24, 2013
Energy Fuels 2013 4th Quarter
Three (3) Stack Filter Sample
47656
CASE NARRATIVE
On December 24, 2013, three stack filter samples were received at TestAmerica's Richland laboratory
for radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification
number as described on the cover page of the Analytical Data Package report form. The samples were
assigned to Lot Number J3L300411.
II. Sample Receipt
The sample was received in good condition and no anomalies were noted during check-in.
III. Analytical Results/Methodology
The analytical results for this report are presented by laboratory sample ID. Each set of data includes
sample identification information; analytical results and the appropriate associated statistical
uncertainties.
The analysis requested was:
Alpha Spectroscopy
Thorium-228, -230, -232 by method RL-ALP-001
Uranium-234, -235, -238 by method RL-ALP-004
Gas Proportional Counting
Pb-210 by method RL-GPC-011
Alpha Scintillation
Radium-226 by method RL-RA-001
IV. Quality Control
TestAmerica Laboratories, Inc. 2
Denison Mines (USA) Corp
January 28, 2014
The analytical result for each analysis performed includes a minimum of one laboratory control sample
(LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments"
section.
V. Comments
Alpha Spectroscopy
Thorium-228. 230, 232
Sample Rl Dryer BH Filter (6099) tracer recovery was above the acceptance limits. A recount confirmed
the high recovery. The batch blank result for Th-230 was above the achieved MDA; it was recounted and
the result is below the MDA. The achieved MDA of the batch exceeds the detection limit from reduced
aliquot sizes taken due to historical process knowledge. There is no sample volume remaining for re-
analysis. Data is reported. Except as noted, the LCS, batch blank and sample results are withi\1
acceptance limits.
Uranium-234. 235. 238
The achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to
historical process knowledge. All of the batch results except for the batch blank and U-235 for sample
R2 SYC Scrubber Filter (6098) exceed the MDAs. Data is accepted. Except as noted, the LCS, batch
blank and sample results are within acceptance limits.
Gas Proportional Counting
Pb-210
The achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to
historical process knowledge. The sample activities exceed the MDAs. Data is accepted. Except as
noted, the LCS, batch blank and sample results are within acceptance limits.
Alpha Scintillation
Radium-226
The achieved MDA of the batch exceeds the detection limit due insufficient sample volume and
limitations ofthe method in relation to the matrix and available count time. There is no sample volume
remaining for re-analysis. Data is repotied. Except as noted, the LCS, batch blank and sample results are
within acceptance limits.
I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically
and for completeness, f-or other than the conditions detailed above. The Laboratory Manager or a
designee, as verified by the following signature has authorized release of the data contained in this hard
copy data package.
TestAmerica Laboratories, Inc. 3
Drinking Water Method Cross References
DRINKING WATERASTM METl-lOD CROSS REFERENCES --
Referenced Method lsotope(s) TestAmerfca Richland's SOP No-.-
I
EPA 901.1 Cs-134, 1-131 RL-GAM-001
EPA 900.0 Alpha & Beta RL-GPC-001
EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002
EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002
EPA 903.1 Ra-226 RL-RA-001
EPA 904.0 Ra-228 RL-RA-001
EPA 905.0 Sr-89/90 RL-GPC-003
ASlM 05174 Uranium RL-KPA-003
EPA 906.0 Tritium RL-LSC-005
Results in this report relate only to the sample(s) analyzed.
Uncertainty Estimation
TestAmerica Richland has adopted the internationally accepted approach to estimating
uncertainties described in "NIST Technical Note 1297, 1994 Edition". The approach, "Law of Propagation
of Errors", involves the identification of all variables in an analytical method which are used to derive a
result. These variables are related to the analytical result (R) by some functional relationship, R == constants * f(x,y,z, ... ). The components (x,y,z) are evaluated to determine their contribution to the overall method
uncertainty. The individual component uncertainties (ui) are then combined using a statistical model that
provides the most probable overall uncertainty value. All component uncertainties are categorized as type
A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the
components, such as sample homogeneity, are combined with the component uncertainty as the square root
of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result
is the combined uncertainty (u0) multiplied by the coverage factor (1,2, or 3).
When three or more sample replicates are used to derive the analytical result, the type A
uncertainty is the standard deviation of the mean value (S/?n), where Sis the standard deviation of the
derived results. The type B uncertainties are all other random or non-random components that are not
included in the standard deviation.
The derivation of the general "Law of Propagation of Errors" equations and specific example are
available on request.
TestAmerlca Inc
rotGenerallnfo v3.72
TestAmerica Laboratories, Inc. 4
-
--
AcUon Lev
Batch
Bias
COCNo
Count Error (#s)
Total Uncert (#s) u, _Combined
Ut~certalnty.
(#s), Coverage
Factor
CRDL(RL)
Lc
Lot-Sample No
MDCIMDA
Primary Detector
Ratio U-234/U-238
Rst/MDC
Rst/TotUcert
Report DB No
RER
SDG
Sum Rpt Alpha
Spec Rst(s)
Work Order
Yield
TestAmerica Inc
l'ntGencrallnfo v3.72
TestAmerica Laboratories, Inc.
Report Definitions
An ngreed upon activity level used to trigger some action when the finnl rc..-;llll L<; greater than or equal to tin: Action
Lev"!. Onen tbll Action Level is relatli(l to the Decision Umit.
The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed
together.
Defined by the equation (Result/Expected)-! as defined by ANSI Nl3.30.
Chain of Custody Number assigned by the Client or TestAmerlca.
Poisson counting statistlcs of the gross sample count and background. The uncet•tainty is absolute and in the same
units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background.
All known uncertainties associated with the preparation and tu1alysis of the sample are propagated to give a measure
of the uncertainty associated with the result, Uc the combined uncertainty. The uncertainty is absolute and in the
same units as the result.
The coverage factor defines the width ofthe confidence interval, 1, 2 or 3 standard deviations.
Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmerica "default"
nominal detection limit. Often referred to the reporting level (RL)
Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
associated with the sample. The Type I error probability is approximately 5%. Lc=( 1.645 •
Sqr!(2•(BkgrndCnt/BkgrndCntMin)/SCntMin)) + (ConvFct/(Eff*Yld*Abn~Vol) * IngrFct). For LSC methods the
batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count
is zero.
The number assigned by the LIMS software to track samples received on the same day for a given client. The
sample number is a sequential number assigned to each sample in the Lot.
Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
with a Type I and II error probability of approximately 5%. MDC= ( 4.65 *
Sqrt((BkgrndCnt/BkgrndCntMin)/SCntMin) + 2.71/SCntMin) * (ConvFct/(Eff * Yld * Abn *Vol)* lngrFct). For
LSC methods the batch blank is used as a measure of the background variability.
The instrument identifier associated with the analysis of the sample aliquot.
The U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural uranium in NIST SRM 4321C is
1.038.
Ratio of the Result to the MDC. A value greater than 1 may indicate activity above background at a high level of
confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers
associated with the result.
Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of2 a value greater than 1 may
indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence
interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers
associated with the result.
Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order
Number.
The equation Replicate Error Ratio= (S-D)/[sqrt(TPUs2+ TPUd2)] as defined by ICPT BOA where S is the original
sample result, Dis the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the
total uncertainty of the duplicate sample.
Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt.
The sum of the reported alpha spec results for tests derived from the same sample excluding duplicate result where
the results are in the same units.
The LIMS software assign test specific identifier.
The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method.
5
Sample Results Summary Date: 28-Jan-14
TestAmerica Inc
Ordered by Method, Batch No., Client Sample ID,
Report No. : 58563 SDG No: 47656
Client ld Tracer
Batch Work Order Parameter Result+-Uncertainty ( 2s) Qual Units Yield MDL CRDL RER2
4002023 RICHRC5011
R1 Dryer BH filter(6099) and b
M2QVR2AA Th-228 · 2.43E-07 +-8.5E-08 uCi/Sample 166% 3.64E-08
Th-230 3.93E-05 +-6.2E-06 uCi/Sample 166% 3.03E~08 3.00E-15
Th-232 3.68E-07 +-1.1 E-07 uCi/Sample 166% 2.83E-08
R1 SYC Scrubber filter(6097) a
M2QVT1AA Th-228 1.67E-08 +-2.1E-OB u uCi/Sample 97% 3.02E-OB
Th-230 1.16E-07 +-5.6E-08 uCi/Sample 97% 2.93E-08 3.00E-15
Th-232 -9.40E-10 +-1.2E-08 u uCi/Sample 97% 2.68E-08
R2 SYC Scrubber filter(6098) a
M2QW1AA Th-228 1.18E-OB +-2.1E-08 u uCi/Sample 80% 4.16E-OB
Th-230 9.56E-07 +-2.3E-07 uCi/Sample 80% 2.87E-08 3.00E-15
Th-232 4.23E-08 +-3.6E-08 uCi/Sample 80% 2.87E-08
4002022 FFSR
R1 Dryer BH filter(6099) and b
M2QVR1AE U-234 1.03E-02 +-1.6E-03 uCi/Sample 99% 2.90E-05 9.00E-15
U-235 4.10E-04 +-1.0E-04 uCi/Sample 99% 1.60E-05 9.00E-15
U-238 1.06E-02 +-1.7E-03 uCi/Sample 99% 2.13E-05 9.00E-15
R1 SYC Scrubber filter(6097) a
M2QVT1AE U-234 8.73E-04 +-2.0E-04 uCi/Sample 95% 5.26E-05 9.00E-15
U-235 3.74E-05 +-3.1E-05 uCI/Sample 95% 3.20E-05 9.00E-15
U-238 9.37E-04 +-2.1E-04 uCi/Sample 95% 4.95E-05 9.00E-15
R2 SYC Scrubber filter(6098) a
M2QW1AE U-234 8.62E-04 +-2.0E-04 uCi/Sample 82% 4.72E-05 9.00E-15
U-235 1.23E-05 +-2.0E-05 u uCi/Sample 82% 4.10E-05 9.00E-15
U-238 9.48E-04 +-2.1E-04 uCi/Sample 82% 3.44E-05 9.00E-15
4002025 RICHRC5011
R1 Dryer BH filter(6099) and b
M2QVR1AD Pb-21 0 2.78E-06 +-5.4E-07 uCi/Sample 82% 3.37E-07 6.00E-14
R1 SYC Scrubber filter(6097) a
M2QVT1AD Pb-210 1.44E-06 +-3.6E-07 uCi/Sample 74% 3.94E-07 6.00E-14
R2 SYC Scrubber filter(6098) a
M2QW1AD Pb-210 1.13E-06 +-3.0E-07 uCi/Sample 87% 3.40E-07 6.00E-14
4002024 RL-RA-001
R1 Dryer BH filter(6099) and b
M2QVR1AC RA-226 1.10E-06 +-2.7E-07 uCi/sample 98% 2.20E-08 9.00E-14
R1 SYC Scrubber filter(6097) a
M2QVT1AC RA-226 5.31E-08 +-2.5E-08 uCi/sample 70% 3.50E-08 9.00E-14
R2 SYC Scrubber filter(6098) a
TestAmerica Inc RER2 -Replicate Error Ratio= (8-D)/[sq•·t(sq(TPUs)+sq(TPUd))] as defined by ICPT BOA.
rptTALRchSaSum U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the MdcJMdn/Mdl, Total Unccrt, CRDL, RDL or
mary2 V5.2.26 not identified by gamma scan softwa1·e.
A2002
TestAmerica Laboratories, Inc. 6
Report No. : 58563
Client ld
Batch Work Order Parameter
4002024 RL·RA-001
R2 SYC Scrubber filter(6098) a
M2QVV1AC RA-226
No. of Results: 24
Sample Results Summary
TestAmerica Inc
Ordered by Method, Batch No., Client Sample I D.
Date: 28-Jan-14
SDG No: 47656
Result+-Uncertainty ( 2s) Qual Units
Tracer
Yield
1.61 E-07 +-5.0E-08 uCI/sample 70%
MDL CRDL RER2
3.55E-08 9.00E-14
TestAmerlca Inc RER2 -Replicate E1·ror Rallo= (S-D)/[sqrt(sq(TPUs)+sq(TPUd))] as defined by ICPT BOA.
rptTALRchSaSum
mary2 V5.2.26
A2002
TestAmerica Laboratories, Inc. 7
QC Results Summary Date: 28-Jan-14
TestAmerica Inc
Ordered by Method, Batch No, QC Type,.
Report No. : 58563 SDG No.: 47656
Batch Tracer LCS
Work Order Parameter Result+-Uncertainty ( 2s) Qual Units Yield Recovery Bias MDL
RICHRC5011
4002023 BLANK QC,
M2Q542AA Th-228 -9.87E-11 +-2.8E-1 0 u uCi/Sample 54% 9.12E-10
Th-230 -1.06E-11 +-2.7E-1 0 u uCi/Sample 54% 5.33E-10
Th-232 O.OOE+OO +· 2. 7E-1 0 u uCi/Sample 54% 3.59E-10
4002023 LCS,
M2Q541AC Th-230 2.38E-08 +-5.1 E-09 J uCi/Sample 86% 106% 0.1 3.22E-10
FFSR
4002022 BLANK QC,
M2Q531AA U-234 9.91 E-08 +-1 .4E-07 u uCi/Sample 93% 2.52E-07
U-235 -1.95E-08 +-8.3E-08 u uCi/Sample 93% 2.41 E-07
U"238 3.74E-08 +-1.4E-07 u uCi/Sample 93% 3.83E-07
4002022 LCS,
M2Q531AC U-234 5.70E-06 +-1.3E-06 uCi/Sample 86% 99% 0.0 1 .97E-07
U-238 5.02E-06 +· 1 .2E-06 uCi/Sample 86% 84% -0.2 2.45E-07
RICHRC5011
4002025 BLANK QC,
M2Q561AA Pb-210 2.28E-07 +-2.1 E-07 u uCi/Sample 88% 3.43E-07
4002025 LCS,
M2Q561AC Pb-210 9.38E-06 +-1 .6E-06 uCI/Sample 92% 104% 0.0 3.20E-07
RL-RA-001
4002024 BLANK QC,
M2Q551AA RA-226 2.27E-08 +-1.7E-08 u uCi/sample 89% 2.47E-08
4002024 LCS,
M2Q551AC RA-226 9.73E-06 +-1 .9E-06 J uCi/sample 100% 96% 0.0 2.38E-08
No. of Results: 13
Bins -(Result/Expected)-1 as defined by ANSI N13.30. TestAmerica Inc
rptSTLRchQcSum
mary V6.2.26
A2002
J Qual-No U or< qualifier lias been assigned and tbe result is below tbe Reporting Limit, RL (CRDL) m· Report Value is Estimated.
U Qual -Analyzed for but not detected above limiting crite1·la. Limit criteria Is less than tile Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or
not Identified by gamma scan software.
TestAmerica Laboratories, Inc. 8
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3 ~ c;·
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r FORM I Q) Date: 28-Jan-14 rr 0 Ql SAMPLE RESULTS Q a;·
-"' 5" Lab Name: TestAmerica Inc SDG: 47656 Collection Date: 12117/2013 2:00:00 PM (.")
Lot-Sample No.: J3L300411-1 Report No.: 58563 Received Date: 12/24/2013 2:00:00 PM
Client Sample ID: R1 Dryer BH filter(6099) and b COC No.: Matrix: FILTER
Enetm;: Fuels 2013 4th Quarter Ordered by Client Sam~le 10, Batch No.
Result Count Total MDL, RptUnit, Yield Rst/MDL, Analysis, Total Sa Aliquot Primary
Parameter Qual Error ( 2 s) Uncert(2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Prep Date Size Size Detector
Batch: 4002022 FFSR Work Order: M2QVR1AE Report DB ID: 9M2QVR10
U-234 1.03E-02 4.1E-04 1.6E-03 2.90E-05 uCi/Sample 99% (357.4) 1110/14 07:09 p 1.0 0.00148 ALP2
8.23E-06 9.00E-15 (12.6) Sample Sample
U-235 4.10E-04 8.1E-05 1.0E-04 1.60E-05 uCi/Sample 99% (25.6) 1/10/14 07:09 p 1.0 0.00148 ALP2
3.73E-06 9.00E-15 (8.) Sample Sample
U-238 1.06E-02 4.1E-04 1.7E-03 2.13E-05 uCi/Sample 99% (498.) 1/10/14 07:09 p 1.0 0.00148 ALP2
<D 5.49E-06 9.00E-15 (12.6) Sample Sample
Ratio U-2341238 = 1.0
Batch: 4002023 RICHRCS011 Work Order: M20VR2AA Report DB ID: 9M2QVR20
Th-228 2.43E-07 7.6E-08 8.5E-08 3.64E-08 uCi!Sample 166% (6.7) 1/20/14 03:14 p 1.0 0.9888 ALP114
9.86E-09 (5.7) Sample Sample
Th-230 3.93E-05 9.4E-07 6.2E-06 3.03E-08 uCi/Sample 166% (1294.5) 1/20/14 03:14 p 1.0 0.9888 ALP114
7.82E-09 3.00E-15 (12.8) Sample Sample
Th-232 3.68E-07 9.2E-08 1.1E-07 2.83E-08 uCi/Sample 166% (13.) 1/20/14 03:14 p 1.0 0.9888 ALP114
7.12E-09 (6.8) Sample Sample
Batch: 4002024 RL-RA-001 Work Order. M2QVRfAC Report DB ID: 9M2QVR10
RA-226 1.10E-06 3.8E-08 2.7E-07 2.20E-08 uCi/sample 98% (50.) 1/22/14 05:35 p 1.0 0.9888 ASC2MA
1.06E-08 9.00E-14 (8.2) Sample Sample
Batch: 4002025 RICHRC5011 Work Order. M2QVR1AD Report DB ID: 9M2QVR10
Pb-210 2.78E-06 2.8E-07 5.4E-07 3.37E-07 uCi/Sample 82% (8.3) 1/23/14 11:08 a 1.0 0.98881 GPC318
1.64E-07 6.00E-14 (10.3) Sample Sample
TestAmerica Inc MDCJMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSample J Qual -No U or < qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated.
VS.2.26 A2002 U Qual ·Analyzed for but not detected above limiting criteria Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
~ ~ !!l c;·
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Lab Name: TestAmerica Inc
Lot-sample No.: J3L300411-1
FORM I
SAMPLE RESULTS
SDG: 47656
Report No. : 58563
Client Sample ID: R1 Dryer BH filter(6099) and b
Enetm' Fuels 2013 4th Quarter
COCNo.:
Result Count Total MDL, Rpt Unit, Yield Rst/MDL,
Parameter Qual Error ( 2 s) Uncert(2 s) Action Lev Lc CRDL(RL) Rst/TotUcert
No. of Results: 8 Comments:
Date: 28-Jan-14
CoUection Date: 12/17/2013 2:00:00 PM
Received Date: 12/24/2013 2:00:00 PM
Matrix: Fll TER
Ordered by Client Sample ID, Batch No.
Analysis,
Prep Date
Total Sa Aliquot
Size Size
Primary
Detector
TestAmerlca Inc MDCJMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSarnple J Qual -No U or< qualifier has been assigned a~~ the ~u_lt is ~el_ow ~e _R~portlng Limit, RL (CRDL) or Report Value Is Estimated. .
VS.2.2S A2002 U Qual-Analyzed for but not detected above llmrting critena. l rmrt critena rs less than the Mdc/Mda/Mdl, Total Uncert, CROL, RDL or not rdentified by gamma scan software.
-I (1) (/) s> 3 ~ (1"
Ill
r FORM I Ill Date: 28-Jan-14 cr 0 Dl SAMPLE RESULTS Q c;;·
!."
:J p Lab Name: TestAmerica Inc SDG: 47656 Collection Date: 12/16/2013 10:00:00 AM
Lot-Sample No.: J3L300411-2 Report No.: 58563 Received Date: 12/24/2013 2:00:00 PM
Client Sample 10: R1 SYC Scrubber filter(6097) a COC No.: Matrix: FILTER
Ene;!}l~ Fuels 2013 4th Quarter Ordered by Client Sample I D. Batch No.
Result Count Total MDL, Rpt Unit, Yield Rst/MDL, Analysis, Total Sa Aliquot Primary
Parameter Qual Error ( 2 s) Uncert(2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Prep Date Size Size Detector
Batch: 4002022 FFSR Work Order: M2QVT1AE Report DB 10: 9M2QVT10
U-234 8.73E--04 1.4E-04 2.0E-04 5.26E..Q5 uCi/Sample 95% (16.6) 1/10/14 07:09 p 1.0 0.0011 ALP3
1.59E-05 9.00E-15 (8.9) Sample Sample
U-235 3.74E..Q5 3.0E-05 3.1E..Q5 3.20E-05 uCi/Sample 95% (1.2) 1/10/14 07:09 p 1.0 0.0011 ALP3
8.43E-06 9.00E-15 (2.4) Sample Sample
U-238 9.37E--04 1.5E..Q4 2.1E-04 4.95E-05 uGVSample 95% (18.9) 1/10/14 07:09 p 1.0 0.0011 ALP3
1.47E-05 9.00E-15 (9.1) Sample Sample
Ratio u-234/238 -0.9
Batch: 4002023 RICHRC5011 Work Order: M2QVT1AA Report DB 10: 9M2QVT10
Th-228 1.67E-08 u 2.1E..Q8 2.1E-08 3.02E..Q8 uCi/Samj:ile 97% 0.55 1/16/14 07:53 p 1.0 0.9894 ALP114
7.59E..Q9 (1.6) Sample Sample
Th,-230 1.16E--07 5.3E-08 5.6E..Q8 2.93E-08 uCi/Sample 97% (4.) 1/16/14 07:53 p 1.0 0.9894 ALP114
7.36E..Q9 3.00E-15 (4.1) Sample Sample
Th-232 -9.40E-10 U 1.2E-08 1.2E-08 2.68E-08 uCi/Sample 97% -0.04 1/16/14 07:53 p 1.0 0.9894 ALP114
6.53E..Q9 -0.16 Sample Sample
Batch: 4002024 RL-RA-001 Work Order. M2QVT1AC Report DB ID: 9M2QVT1 0
RA-226 5.31E-Q8 2.3E..Q8 2.5E..Q8 3.50E-08 uCVsample 70% (1.5) 1/22/14 05:35 p 1.0 0.9888 ASG3MA
1.69E..Q8 9.00E-14 (4.2) Sample Sample
Batch: 4002025 RJCHRC5011 Work Order. M2QVT1AD Report DB ID: 9M2QVT10
Pb-210 1.44E-06 2.7E-07 3.6E..Q7 3.94E..Q7 uCVSample 74% (3.6) 1/23/14 11:08 a 1.0 0.9894 GPC31C
1.92E--07 6.00E-14 (7.9) Sample Sample
TestAmerica Inc MDCjMD.A,Lc-Detection, Decision Level based on instrument background or blank. adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSample J Qual -No U or< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated.
y 52_26 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
---------------------------------... -----------· --··-·----
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......
N
FORM I
SAMPLE RESULTS
Date: 28-Jan-14
Lab Name: TestAmerica Inc
Lot-sample No.: J3L300411-2
Client Sample ID: R1 SYC Scrubber filter{6097) a
SDG: 47656
Report No. : 58563
COCNo.:
Collection Date: 12/16/2013 10:00:00 AM
Received Date: 12/24/2013 2:00:00 PM
Matrix: FILTER
Energy Fuels 2013 ~-t!!_ Quarter Ordered by Client Sample 10. Batch No.
Result Count
Parameter Qual Error ( 2 s)
No. of Results: 8 Comments:
Total MDL, Rpt Unit,
Uncert( 2 s) Action Lev Lc
Yield Rst/MDL,
CRDL{RL) Rst/TotUcert
Analysis,
Prep Date
TestAmerlca Inc MDCIMDA.Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
Total Sa
Size
Aliquot
Size
Primary
Detector
rptSTLRchSam. 1e J Qual -No U or < qualifier has been assigned and the result is below the Reporting Umit, RL (CRDL) or Report Value Is Estimated.
VS.2.2S A2002 p U Qual -Analyzed for but not detected above limiting criteria. Umit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not Identified by gamma scan software.
-I CD "' ~ 3 9l c;·
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r FORM I Ql Date: 28-Jan-14 CY 0 Ql SAMPLE RESULTS Q ffi' -"'
3" Lab Name: TestAmerica Inc SDG: 47656 Collection Date: 12117/201311:00:00AM r>
Lot-sample No.: J3L300411-3 Report No.; 58563 Received Date: 12/24/2013 2;00:00 PM
Client Sample ID: R2 SYC Scrubber filter(6098) a COCNo.: Matrix: FILTER
Ena!m: Fuels 2013 4th QuartE!r .Ordered by Client Same!e ID, Batch No.
Result Count Total MDL, Rpt Unit, Yield Rst/MDL, Analysis, Total Sa Aliquot Primary
Parameter Qual Error ( 2 s) Uncert(2 s) Action Lev Lc CRDL(RLJ Rst/TotUcert Prep Date Size Size Detector
Batch: 4002022 FFSR WorkOrder: M2QW1AE Report DB 10: 9M2QW10
U-234 8.62E-04 1.4E-04 2.0E-04 4.72E-05 uCi/Sample 82% (18.3) 1/10/14 07:09 p 1.0 0.0013 ALP4
1.38E-05 9.00E-15 (8.7) Sample Sample
U-235 1.23E-05 u 2.0E-05 2.0E-05 4.1 OE-05 uCi/Sample 82% 0.3 1/10/14 07:09 p 1.0 0.0013 ALP4
1.16E-05 9.00E-15 (1.2) Sample Sample
U-238 9.48E-04 1.5E-04 2.1E-04 3.44E-05 uCi/Sample 82% (27.6) 1/10/14 07:09 p 1.0 0.0013 ALP4
~ 9.20E-06 9.00E-15 (9.) Sample Sample "' Ratio U-2341238 = 0.9
Batch: 4002023 RICHRC5011 Work Order: M2QW1AA Report DB 10: 9M2QW10
Th-228 1.18E-08 u 2.1E-08 2.1E-08 4.16E-08 uCi/Sample 80% 0.28 1/16/14 07:53 p 1.0 0.985 ALP115
1.09E-08 (1.1) Sample Sample
Th-230 9.56E-07 1.7E-07 2.3E-07 2.87E-08 uCi/Sample 80% (33.3) 1/16/14 07:53 p 1.0 0.985 ALP115
6.68E-09 3.00E-15 (8.1) Sample Sample
Th-232 4.23E-08 3.5E-08 3.6E-08 2.87E-08 uCi/Sample 80% (1.5) 1/16/14 07:53 p 1.0 0.985 ALP115
6.68E-09 (2.4) Sample Sample
Batch; 4002024 Rl-RA-001 Work Order. M2QW1AC Report DB 10: 9M2QW10
RA-226 1.61E-07 2.6E-08 S.OE-08 3.55E-08 uCi/sample 70% (4.5) 1/22/14 05:36 p 1.0 0.985 ASCJUA
1.72E-08 9.00E-14 (6.5) Sample Sample
Batch: 4002025 RICHRC5011 Wo.rk Order: M2QW1AD Report DB 10: 9M2QW1 0
Pb-210 1.13E-06 2.3E-07 3.0E-07 3.40E-07 uCi/Sample 87% (3.3) 1/23/1411:08 a 1.0 0.985 GPC31D
1.66E-07 6.00E-14 (7.5) Sample Sample
TestAmerica Inc M"DCJMDA,Lc-Detection, Decision l.e.wl based on lrn.-trument background or blank, adjLIStod by Che sample Efficiency, Ylold, and Volume.
tSTLRchSam le J Qual ·No U or< qualifier has been assigned and the result is below the Repor1fng Wmit, Rl. (CROLl or Repo!'l; Value 1$ Estlma.ted. ~.2.26 A2002 P U Qual· Analyzild for but n9t detected above llmltlf19 criteria. Limit diteria h; II?SS than ttte Md~cla!Mdl, Total Uncert, CRDL, ROL or not Identified by gamma scan software.
~ ~ 3 ~ n·
Ql
r Ql 0" 0 iil 0 ffi·
!!'
:l ~
...... .j>.
Lab Name: TestAmericalnc
Lot-Sample No.: J3L300411-3
Client Sample 10: R2 SYC Scrubber filter(6098) a
FORM I
SAMPLE RESULTS
SDG: 47656
Report No. : 58563
COCNo.:
Date: 28-Jan-14
Collection Date: 12/17/2013 11:00:00 AM
Received Date: 12/24/2013 2:00:00 PM
Matrix: FILTER
Energy Fuels 2913 4th Qu~rter Ordered by Client Sample ID, Batch No.
Result Count Total MDL, Rpt Unit, Yield Rst/MDL, Analysis, Total Sa Aliquot Primary
Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst!TotUqlrt Prep Date Size Size Detector
No. of Results: 8 Comments:
TestAmerica Inc MDC(MDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSample J Qual-No U or< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. vs.2.26 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
-·---------. ____ ,, __ -··---··-----------·-··--~~--------------
-I (1)
"' s> 3 !!l ()"
Ill r Ill FORM II C" a Date: 28-Jan-14 Ql
Q BLANK RESULTS iii' 5I'
5 " Lab Name: TestAmericalnc SDG: 47656
Matrix: FILTER RepQrt No.: 58563
Count Total MDL, Rpt Unit, Rst/MDL, Analysis, Total Sa Aliquot Primary
Parameter Result Qual Error ( 2 s) Uncert(2 s) Lc CRDL Yield Rst/TotUcert Prep Date Size Size Detector
Batch: 400202S RICHRC5011 WorkOrder: M2Q561AA Report DB ID: M2Q561AB
Pb-210 2.28E-07 u 2.1E-07 2.1E-07 3.43E-07 uCi/Sample 88% 0.67 1/23/14 11:08 a 1.0 1.0 GPC32A
1.67E-07 6.00E-14 (2.1) Sample Sample
Batch: 4002024 RL-RA-001 Work Order: M2Q551AA Report DB 10: M2Q551AB
RA-226 2.27E-08 u 1.SE-08 1.7E-08 2.47E-08 uCi/sample 89% 0.92 1/22/14 OS:36 p 1.0 1.0 ASCLMA
1.19E-08 9.00E-14 (2.7) Sample Sample
Batch: 4002022 FFSR Work Order: M2Q531AA Report DB ID: M2Q531AB
01 U-234 9.91E-08 u 1.4E-07 1.4E-07 2.S2E-07 uCi/Sample 93% 0.39 1/10/14 07:09 p 1.0 0.15 ALPS
6.82E-08 9.00E-1S (1.4) Sample Sample
U-235 -1.95E-08 u 8.3E-08 8.3E-08 2.41E-07 uCi/Sample 93% -0.08 1/10/14 07:09 p 1.0 0.15 ALPS
6.44E-08 9.00E-15 -0.47 Sample Sample
U-238 3.74E-08 u 1.4E-07 1.4E-07 3.83E-07 uCi/Sample 93% 0.1 1/10/14 07:09 p 1.0 0.15 ALPS
1.16E-07 9.00E-15 O.S2 Sample Sample
Ratio U-2341238 = 2. 7
Batch: 4002023 RICHRC5011 Work Order: M2Q542AA Report DB ID: M2Q542AB
Th-228 -9.87E-11 u 2.8E-10 2.8E-10 9.12E-10 uCi/Sample 54% -0.11 1/22114 10:01 a 1.0 99.26 ALP401
2.53E-10 -0.7 Sample Sample
Th-230 -1 .06E-11 u 2.7E-10 2.7E-10 5.33E-10 uCi/Sample 54% -0.02 1/22/14 10:01 a 1.0 99.26 ALP401
1.24E-10 1.00E+OO -0.08 Sample Sample
Th-232 O.OOE+OO u O.OE+OO 2.7E-10 3.S9E-10 uCi/Sample 54% 0. 1/22/14 10:01 a 1.0 99.26 ALP401
8.84E-11 0. Sample Sample
No. of Results: 8 Comments:
TestAmerica Inc MDCJMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, a.nd Volume.
rptSTLRchBiank U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
V5.2.26 A2002
~ ~ 3 ~ n· "' r "' C" 0 iil Q n;·
C/)
:J ,
..... (J)
Lab Name: TestAmerica Inc
Matrix: FILTER
Parameter Result
Batch: 4002025 RICHRC5011
Pb-210 9.38E-06
Batch: 4002024 Rl-RA-001
RA-226 9.73E-06
Batch: 4002022 FFSR
U-234 5.70E-06
U-238 5,02E-06
Batch: 4002023 RICHRC5011
Th-230 2.38E-08
No. of Results: 5 Comments:
Count
Qual Error ( 2 s)
3.8E-07
1.1 E-07
9.2E-07
8.6E-07
2.8E-09
FORM II
LCS RESULTS
SDG: 47656
Report No. : 58563
Total
Uncert(2 s)
Report
Unit
Expected Recovery,
MDL Yield Expected Unce;rt Bias
Work Order. M2Q561AC Report DB ID: M2Q561 CS
1.6E-06 3.20E-07 uCi/Sample 92% 9.01 E-06 1.53E-07 104%
Rec Limits: 20 115 0.0
Work Order: M2Q551AC Report DB ID: M2Q551 CS
1.9E-06 2.38E-08 uCifsample 100% 1.01 E-05 1.03E-07 96%
Rec Limits: 70 130 0.0
Work Order: M2Q531AC Report DB ID: M2Q531CS
1.3E-06 1.97E-07 uCi/Sample 86% 5.73E-06 1.77E-07 99%
RecLimits: 70 130 0.0
1.2E-06 2.45E-07 uCi!Sample 86% 6.00E-06 1.85E-07 84%
RecLimits: 70 130 -0.2
Work Order: M2Q541AC Report DB ID: M2Q541 CS
5.1E-09 3.22E-10 uCi/Sample 86% 2.26E-08 2.34E-10 106%
Rec Limits: 70 130 0.1
Analysis,
Prep Date
1/23/14 11:08 a
1/22/14 05:38 p
1/10/14 07:09 p
1/10/14 07:09 p
1/16/14 07:53 p
TestAmerica Inc Bias -(Result/Expected}-I as defined by ANSI Nl3.30.
rptSTLRchLcs
V5.2.26 A2002
Date: 28-Jan-14
Aliquot
Size
1.0
Sample
1.0
Sample
0.17
Sample
0.17
Sample
99.59
Sample
PrlmaJy
Detector
GPC32B
ASCNMD
ALPS
ALP6
ALP23
-I CD "' )>
3 ~ c;·
Q)
r Q) 0" 0 Dl Q
Cii"
"' :::> ,
~
-.J
Chain of
Custody Record
"'I)\L4~(100ll
C5ltll
Tetco
Address 391 East 620 South
Ctly . k Amencan For 1
SlstJJ ~Zii>~
Ut 84003
P1cfi.lc1-N:Jft'.e 111111 Local""' .'Siil.iii/
Entl!ID'_Fuels 2013 4th Quarter
~:PL~ Otr!t!r/CJWCgNo.
Temperatllre on Receipt __ _
Drinking Water? Yes 0 No 0
Prr>Jr;.aMM~
Dean Kitchen
7lit"'PP>>OO tojUitltlbr(l.re;J. C".DIAl)JFuNurnber.
801-492-9106
I S<le Contact l Lab Coo/act
Scott Ouin.nsen, G•rn:n P•lmer
,C.~Il'\'>'~fV~
Matrix
Test America
THE LEADER IN ENVIRONMENTAL TESTING
Date
12/18/2013
Lab Number
Analysts (Ati,lCh list if
more space is n_eeded)
~ I~ 0 ~ ~ ~
Sample /.D. No. and Description ± ~ m
(Containats for each sample may be combined on one line) ...... .....~
R1 Dryer BH filter(G099) and beaker i 12/17/13 14:00 X X1x1x1x
R1 SYC Scrubber filter (6097) and beaker 12/16/13 10:00 xl XIJ.<IX I X
R2 SYC Scrubber filter t6098l and be<tker 12/17/13 11:00 X X1x1x 1x
_:s'>::>L'~~
~ .. -\;\ "'vf5~
~-\-3\-\"'h_
-~I ~lllllllllllllllll illllllll -:13(300411
Cltnln or CUS~D:JY Mlmb6'
Pa~ l of J
Special Instructions!
Conattions of Receipt
lY'\ ~ (;) "\) \(
t"\ ';\. ~-J "' I M'A~..Jv .....
0 Unknovm ~~==tent PCssi/JJa HSZ91fJ. hf.Stiii6Cliut;<t
0 Non-Hazard 0 Flammable 0 Skin lnilant
(.1\ fee may ba assesserJ if semp/es are retained 0 DI>'{Josal By Lab 0 ArChive For ___ MDnlhs longer than 1 mo!llh) 0 PoisonS
T./m,~T...,.,Frsqairod cc fi~---(SjiiiiWJ 0 24 Hours 0 48 Hours 0 T Days 0 14 Days 0 21 Days . as oer method.... ___ .
~;::jc .
.:1-~:By
COtnmonts
When Complete Email to: Dean or Paul [e-mail]
biSTRISili1lW: W/11TE.-Ririliiiiii:f!J> ctfiiiiinilh ltD~ CANMi'f-St.)'$ "'lh lf>t~ PIN!<• -C<Jplf
Test America
THe LEAOI!R IN ENVIRONMENlf<.L TESTIN<3 )
Date/Time Received: /j). ... J 4-/);o/1 r y ':.0 ~
Sample Checl(-in List
Container GM Screen Result (Airlock) ~ 0
Sample GM Screen Result (Sample Receiving) $0
cpm Initials(b,( ]
cpm Initials[/.) .1]
Client: J E T ( 0 L~f:0 J SDG #: "-V"\\oS\...o
Lot Number: :S?i1::©C>'A\\
SAF #: ________ ____.NA~~]
ChainofCu~ody# ____________________________________________________________________ ___
Shipping Container ID or Air Bill Number : _________________ NA i? ]
Samples received inside shipping container/cooler/box Yes [jj/] Continue with 1 through 4. Initial appropriate response.
No [ ] Go to 5, add comment to #16.
1. Custody Seals on shipping container intact?
2. Custody Seals dated and signed?
Yes [ ] No [ No Custody Seal ()"//]
Yes [ ] No[ No Custody Seal [p-I]
3. Cooler temperature: _oc NA ~~~]
4. Vermiculite/packing materials is NA rP//J Wet[ ] Dry[
Item 5 through 16 for samples. Initial appropriate response.
5. Chain of Custody record present? Yes [5>//] No [
6. Number of samples received (Each sample may contain multiple bottles):. ____ .o<..,. _______________ _
7. Containers received: 3 X f3 £. tf /( ( ('{ 1 3 X FJ l TE 1-.
8.
9.
10.
11.
12.
13.
14.
15.
16.
Sample holding times exceeded? NA [{1.. ] Yes [ ] No [ ]
Samples have: tape hazard labels ____ custody seals IJI/ appropriate sample labels
Matn.'x: _)jf__ A (JiLT, Wipe, Solid, Soil) ___ I (Water) __ S (Air, Niosh 74~ T (Biological, Ni-63) sa;npl~: ~ \1--~~c. ·--, -v
_.uJif_ru-e In good condition ___ ru·e leaking __ are broken
__ have air bubbles (Only for samples requiring no head space) ___ Other---=----------
Sample pH appropriate for analysis requested Yes [ ] No [ ] NA rPif J
(If acidification is necessary go to pH area & document sample ID, initial pH, amount of HN03 added and pH after addition on table)
Were any anomalies identified in sample receipt? Yes [ ] No '1/)-/(]
Description of anomalies (include sample numbers): NA ~:, ] -------------------------
Sample Location, Sample Collector Listed on COC? *
*For documentation only. No cotTective action needed.
Yes ] No [
Additional Information: _________________________________________ _
] Client/Courier denied temperature check. ] Client/Courier unpack cooler.
S~mple Ch~¥~le~~~!lto-dian: Slgnmure:....,r~=""'-~~~=-o..-=--------==-------------Date/J-~ lj -~I '3
Client Notification needed? Yes [ ] No [ Date:
By:
Person contacted:
[~No action oecessory; p:cess as ih _,... ~ f
ProjectM"nsger z,~. .rL c~-rJ ~ Dure r?.....:-'~1 -1 ~
LS-023 Rev. 17,05113 Page 1 of-+
TestAmerica Laboratories, Inc. 18
APPENDIXD
South Yell ow Cake Scrubber
Figure 1. Facility Schematic Representation
Yell ow Cake Dryer Baghouse
Figure 2. Facility Schematic Representation
Process Data
(Retained by Energy Fuels Resources)
D
Facility, Energy Fuels Resources
t
a
~
y
Stackldentification: South yellow Cake Scrubber
1~0~1
~
a: Distance upstream from next disturbance, feet -----
~: Distance downstream from last disturbance, feet
y: Distance of Sample Level to Ground, feet _
0: Stack Inside Diameter, inches --
Estimated Moisture, percent
Estimated Temperature, "F -----
Estimated Velocity, fpm _-....:·:....-___ _
Control Unit
Type:
Scrubber
Number of Ports
!If
Figure 1. Facility Schematic Representation
Process
Type:
Yell ow Cake Processing
FociHty, Energy Fuels Resources
t
a
!
y
stackidentification: Yellow Cake Dryer Baghouse
1~0~1
~
a: Distance upstream from next disturbance, inches
~: Distance downstream from last disturbance, inches
y: Distance of Sample Level to Ground, feet
0: Stack Inside Diameter, inches
Estimated Moisture, percent
Estimated Temperature, °F
Estimated Velocity, fpm ___
Control Unit
Type:
Baghouse
Number of Ports 2
~
57"
454"
65'
16"
0-2%
125
1,400
Figure 2. Facility Schematic Representation
Process
Type:
Yell ow Cake Processing
Energy Fuels Resources, Blanding, UT Process Data
Source: South Yellow Cake Date : I; --lr/ --/)
Scrubber Flow GPM
Time #1 #2 6P
Cf: J 0 I{,· 3 3o ·1-to ·t
I 0' o o [&.~ 3o·<t I 0 ·1
to_· 30 {~~.) 3o-7-I o-1
l ( ' o b ( 0-s-3D ·1-)0 ·1
11 • :5 () I~. s-3D· ~r-I u·1
ll_ I DO (to . .__( '30. + I o · ·f ,
IZ.,'3o I cP -S" 3D·<(-\ () ·1
I 5' Do (+· () 3 0. s-· I o ·1
I!>· 30 I -:J-. 0 3 () . --1--IO ·t
1-7-· I<-(' Oc)
( ~-' ~5 D · s-({)·--::}
I'/,' 3D I ':f . I 30. <6--to -1-
1). OD r 1· I 30· ~ /o ·+
1 s-. 3D ( 1-f 36· 1 1o<f
-n;: 00 11-.o 3 o·r (c) ·1
I(.: 3D l1-· I }o·J (o .·+
1~.' OD It · I ") 0 . .....,._ I D·-::J
1r: 36 11-1 3v-~ IV . r
Energy Fuels Resources, Blanding, UT Process Data
!
Source: South Yellow Cake Date: ' I ·;· I~ ! ,.
J' Scrubber Flow GPM
Time #1 #2 t,P
I t _,;, .~ IG 0 ') (). ¥ [c) ·~
i I ~D I L, · u :~o ... ~ ( ;:>--:]_
I? l~ (_) i(.;. w -;;o -S i u-·J
I 7 l. ~ {) rL '1 _:;: 0. "7 ( (_)' 1
? () I \ ·-J '3: ~~ (.) I ( -~ (). --
i 0
IJ: )b It? ~ '3 (..) ~ / 0 -·J
.• /') =~ I t.l oo -S ~()-~ I I I
[·' v
I "( 30 /Lr 8' ...., If'. :::) £~o-r> ~" j' . \..1
rs· L'· (_) i . c:, 0 0-~l [ l)· -~ LO '
I )--~() I{;~ ·S' ·z;o ·~ I G -·1
n) 01.) 01 '7 . /
( 0· ·i f (o ' '7 l) .. ~
I~· -~ 0 I -·1 -so ··y (0· -~~ ·-+--jl:. . I
I 1 () l.) { C:, ' ~ ~D ( I 0· ·:1 0
I 1 ~ ~~ (.;; ... :7 3D·¥ j()· ·-+
I )) . vD I/.,. G ·) . y ··J 11..-') () I l) L ( ..
I <'( ," 2D 1 lP· c) '') ¥ [) . ·-J / )() l
I 'i : (.J () I G .. C' ) ., ) s ~) {... . ' I o. 1
I I: 3 0 \ ~-s ''){) --~~ \ u-1 '). -
z () . ()()
I
APPENDIXE
Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature
sensors were carried out in accordance with the procedures outlined in the Quality Assurance
Handbook. The appropriate calibration data are presented in the following pages. The nozzle
calibrations are recorded on the first page of the field data sheets.
Figure 3 Schematic of Method 5/114 Sampling Train
Meter Box Calibration Data and Calculations Forms
Post-test Dry Gas Meter Calibration Data Forms
Type S Pitot Tube Inspection Data
Sample Box Temperature Sensor Calibration
E
Temperature Sensor
t ~Probe
TypeS Pitot
Tube
Temperature
Nozzle 1-t<i T.a:::e:l
Sensor~ Gooseneck l .
~ G'a:s4irm
.............. ---...
/
TypeS Pitot
Tube
/ RUe
~
Temperature
Sensor
Glass Filter
Holder
Heated Area
lmpingerTrain Ql!ional, May Be Replaced Sf An EquiValent Condenser
J
Stack
Wall Manometer Temperature Water
Sensor}. Empty Silica
Gel
Orifice
Dry Gas
Meter
Air-Tight
Pump
Figure 3 Schematic ofMethod 5/114 Sampling Train
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Select three critical orifices io calibrate the dry gas meter which bracket the expected operating range
2) Record barometric pressure before and after calibration procedure.
'a ·nm·ii·llta&M®i~= .. __ . ·~ ;:;~ ~ -~~-~~ ti -.:) ~ .., "
JO •
0
G
G
3) Run at tested vacuum (from Orifice Calibration Report). for a period of time
necessary to achieve a minimum total volume of 5 cubic feet.
4) Record data and information in the GREEN cells. YELLOW cells are calculated.
K'
METER SERIAL It:~
CRITICAL ORIFICE SET SERIAL#:~
TESTED
EQUIPMENT ID #:
RUN#
FACTOR ]VACUUM
(AVG) (in Hg)
l
3
2
0.8.137
0.8137
0.8137-
0.5317
0.5317
0.5317
0.3307
0.3307
0.3307
1.2 728.375
12 737 .. 588
12 750.681
12 I 707.497
12 I 714.208
1!.__ I _EO.~
12 689.425
12 694.924
12 701.978
737.588
750.681
768.774
714.208
720.23.5
7~
694.924
701.578
707.497 -
9.213
13.093
18.093
6.711
6.027
8.140
5.499
7.054
5.519
71 74
71 75
71 80
71 73
71 73
71 74
71 73
71 75
____II__ _73_
USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
81
86
92
73
79
81
75
80
76
75 86
80 92
80 90 I
73 79
74 81
74 81
75 80
73 76
72 78 --
DGM
AVG
79
83.25
85.5
74.50
76.75
77.50
75.75
76.00
74.75
FINAL
Lruo]
ELAPSED
TIME(MIN)
9
8.50
12.00
15.50
9.50
8.50
11.50
12.50
15.00
12.50
AVG(P,.,)
25.40
§ 43
3
7.7273
!Mill
~
5.6485
~
6.8129
4.6073
~
lllli
2014 Pre-Calibration
IF Y VARIATION EXCEEDS 2.00%,
ORIFICE SHOULD BE RECALl BRA TED
l
~ 0.987
10.7661 !!&M
14.8034 QJll
AVG• QJll 0.02
5.5693 Q,lli
~ Q,lli
6.7418 ~
AVG= l!&E 0.01
~ M!i
~ ~
~ 0.984
AVG= 0.987 -0.03
The following equations are used to calculate the standard volumes of air passed through the DGM, v. (std), and the cri!ical
or~ice. V0 (std), and lhe DGM calibration factor, Y. These equations are automatica!y calculated in lhe spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = [ 0.987 -~
(1)
(2)
(3)
I'm,.,,,.= K1 *I'm * Pbar+(LIH !13.6)
J'nr
l'cr = K'~ Pbar • ~
'''"' .JTamb
= Net volume of gas sample passed through DGM, corrected to standard conditions
K,; 17 64 'Riin. Hg (English). 0.3358 'Kimm Hg (Metric)
T m = Absoluls DGM avg temperature ('R -English 'K-Metric)
= Volume of gas sample passed through the cntical onfice corrected to standard conditions
T .,r.>ll = Absolute arnbienl temperature (''R-English. ~K-Metric)
K' = Average K' factor from Critical Orifice Calibration "~:.::'..:. ,., = DGM calibration factor
AVERAGE .1H@ =I 1.620 I
t.H . = @
(
0.75 6 )2 :.H {Y_ •• {sld))
V"(std) \ v ...
Temperature Sensors
Reference In Out
OF OF OF
33
58
202
33
67
202
33
68
202
PRE Console #6 Calibration 2014
1JQQ.
1.686
~
!,ill
!&!§.
~
1.,ill
1.,ill
1ill
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
~ .. _ 9 i*flh.Wil#iffiMRMQIIMI!'~ ::: ::< --
1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range,
2) Recond barometric pressure before and after calibration procedure
3) Run at tested vacuum (from Orifice Calibration Report). for a period of time
necessary to achieve a minimum total volume of 5 cubic reeL
4) Record data and information in the • 'cens. YELLOW cell> are calculated.
CRITICAL ORIFICE SET SERIAL "•t ..... 1 EQUIPMENT 10 #:
K' TESTED
,-----r----1 FACTOR I VACUUM
0
G
G
RUN# I IAVG)
l
1
3_
~
3
0.8137
0.8137
0.8137
0.5317
0.5317
0.5317
0.3307
0.3307
0.3307
linHgl
13
13
13
13
13
13
13
13
fJ
I
I
911.2310
919.529
92G.157
870.880
87U22
882.542
868.7010
893.990
899.307
USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
919.529
926.157
932.829
893.990
899.307
904.649
8.298
6.628
6.672
5.642
6.020
5.690
5.289
5.317
5.342
69 85
n 89
68 89
69 75
&9 76
59 78
69 78
69 79
~-82
88 92
89 95
92 97
76 75
78 80
78_ 85
79 81
82 85
_!!__ L_87
FINAL
I zs.zo I
ELAPSED
OGM
AVG
95 90
97 92.25
99 94.25
80 76.50
85 I 79.75
89 I 82.50
85 I 80.75
97 I 83.25
87 1 84.75 12.00
ENVIRONMENTAl SUPPLY COMPANY
2013 Pre-Calibration Console 7
AVG jP,.,)
25.20
6.7732
5.3880
~
4.5946
~
4.6821
4,3563
4.3592
4.3677
IF Y VARIATION EXCEEDS 2.00%.
ORIFICE SHOULD BE RECALIBRATED
1
6.6895 ~
5.3508 Ull
5.3558 !!,lli
AVG= !!,lli_ ·11.36
4.6618 2.ill.
4,Ul2 0.995
4.6618 ~
AVG= 0.995 !!M
4.3493 0.998
4.3493 0.998
4.3493 ~
AVG = Yll ~
M£
M!Q
~
.hill.
1.713
w.!
Lill
1.650
~
The ionowing equanons ore used to calculate the standard volumes oi air passed through the DGM, Vm (s!d) and the critical orifice.
Va (std), and the DGM canbration faclor, Y. T~ese equations are automaticaly calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y = ,--0.994 I
(1)
(2)
(3)
I'm,.,,,~ K, •I'm• Pbar+i~lf 13.6)
Tm
I·< 1 ,1_1 , ::;::;; K ~. l~h_t~r .. (-) Ji'wnh-
= Net volume of gas sample passed through DGM1 corrected to standard conditions
K, = 17 64 'Riin Hg (English) 0 JB58 'Kimm Hg (Meiner
T"' = Absolute DGM a.vg temperature ("R ·English °K-Metric)
= Volume of gas sample passed through the critical orifice. corrected to standard conditions
T 3frO = Absolute arnbi5!nt tempere.tur9 {~R-Engl1sh 9K-Metnc)
K' =-Average K' factor from Cnheal Onftc.e Callbr3tion f'et
I'm.
= DGM calibration factor
AVERAGE ~H~ =j ----u34 ]
aH~= 2
( lbitl ) aH (Vm(std))
V,(s!d) v'"
Temperature Sensors
Reference In Out
"F
32
72
201
OF
33
73
202
OF
33
73
2i.l:!
7 console Pre 2013
•a----"_-·-..··--.,-1~ .. !!!~~
·l '
METHOD 5 DRY GAS METER CALl BRA TION USING CRITICAL ORIFICES
1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.
2) Record barometric pressure before and after calibration procedure.
::J) Kun at teste<l vacuum (tram Unt1ce ~a11orat10n Keport), Tor a peno<l or t1me
necessary to achieve a minimum total volume of 5 cubic feet
4) Record data and information in the GREEN cells, YELLOW cells are calculated.
METER SERIAL II:~
CRITICAL ORIFICE SET SERIAL Jl:~
K' TESTED
FACTOR 'VACUUM I I RUN# I (AVG) (In Hg)
G: 0.5317 16
0.5317 16
0.5317 16
432.310 437.640
437.640 443.318
443.316 455.065
G 1 0.6808 11 EE
2 0.6808 11 .
3 0.6808 11
D:ffiEE
USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
5.330
5.676
11.749
.0
.0
.0
.0
.0
.0
EQUIPMENT ID #:
60 71 71 71 77
60 71 77 73 82
60 73 82 77 86
;] AVG
72.5
75.75
79.5
FINAL
[ 25~5-l
ELAPSED
ITIME
9
!MINJ
7.50
8.00
16.50
AVG(P...,)
25.45
~
1.20
F I I I _I I :: § ~::
I I J_j I I :: § §
[:;
4.5118
4.7755
2.,!@
Denison Mines
IF Y VARIATION EXCEEDS 2.00%,
ORIFICE SHOULD BE RECALIBRATED
1
~ 0.987
~ 0.994
~ ~
AVG= 0.993 Q.Ql!
AVG=
AVG=
The following equatiors are used to calculate the standard volumes of air passed through the DGM, V m {std), and the crilical
orifice, Va (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = r D--:993 -]
(1)
(2)
(3}
Vm, __ .,,,, = K, * Vm * Pbar _ , _ --·-.
Pbar *G -K'* Vcr,_,dJ -.JTamb
= Net volume of gas sample passed through DGM, corrected to standard conditions
K, = 17.64 'Riin, Hg (English), 0.3858 'Kimm Hg (Metric)
T m = Absolute DGM avg. temperature ("R-English, 'K-Metric)
= Volume of gas sample passed through the critical orifice, corrected to standard conditions
T,.,.. = Absolute ambient lemperature ('R-English, 'K-Metric)
K' = Average K' factor from Critical Orifice Calibration Vc~st.ll Y= ,~-= DGM calibration factor
~mt lt.tr
AVERAGE.O.Hg=~LUE! I
.o.H~ = ( 0.75 6 )
2
6H (Vm(std))
V0,(Std) Vm
Temperature Sensors
Reference In Out
OF OF "F
33
67
121
34
66
120
34
66
120
Post test Console #6 2014
1.622
ug
1.601
##111#1#11
l#lfiH#
tl#ltl#ll#
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.
2) Record barometric pressure before and after calibration procedure.
'='--... •'-i<:":?-~ -!!~;,
I ,
3) Run at tested vacuum (from Orifice Calibration Report), for a period of time
necessary to achieve a minimum total volume of 5 cubic feet. Facility simplot 400
4) Record data and information in the <.H ii.9-; cells, YELLOW cells are calculated.
METER SERIAL ''I gguo~ I
CRITICAL ORIFICE SET SERIAL~~ 14535
K' TESTED
RUN#
FACTOR I VACUUM
(AVG) (in Hg)
0:
o:rn~
o:rn~
0.6606 13
0.6608 13
0.6808 13
783.151 789.608
789.608 798.115
796.115 803.116 ----
USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
6.457
6.507
7.001
.0
.0
.0
.0
.0
.0
EQUIPMENT ID II:
60 70 77 75 82
60 75 82 78 86
60 78 86 76 86
§ II II
f-I I I I I
DGM
AVG
7S
80.25
82
0.00
0.00
0.00
0.00
0.00
0.00
FINAL
I 25.45 I
ELAPSED
TIMEIMitol)
e
§ 00
0
AVG(P .. ,)
25.45
§§
§§
5.4442
~
5.8374
IF Y VARIATION EXCEEDS 2.00%,
ORIFICE SHOULD BE RECALIBRATED
1
5.3203 0.977
5.3203 .!l.!!Z
5.7003 0.977
AVG= .!l.!!Z Q,_Qg_
AVG=
AVG=
The following equations are used to calculate the standard volumes of air passed through the DGM, V .. (std), and the critical orifice,
V ~ (sld), and ltle OGM calrbralion factor, Y. These equa~ons are automatically calculated in the spreadsheet abov€. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = [ o.si7)
(1}
(2)
(3)
Vm,_,,,, = K, • Vm • Pbar+ [I'.H 113.6)
Tm = Net volume of gas sample passed through OGM. corrected to standard conditions
K1 = 17 64 'Rirn. Hg (English) 0 3858 'Kimm Hg (Metric)
T m = Absolute OGM avg temperature (0R -Engl1st"1, °K-Metric)
=Volume of gas sample passed through the critical orifice, corrected to standard conditions
T aml:l = Absaiute ambient temperature {0R-Engf1sh, °K-Metric}
K = Average K' factor from Cntical Orifice Calibration Vc1:,.-~, Y=-----Vm p,/,
= OGM calibration factor
AVERAGE 6Hg=l 1. 71 I
2
6H® = ( 0.75 9 ) 6H (Vm(std))
V0,(Std) Vm
1.72
1.71
121
7 console Post Test 2013
typeS l'itot T11hc Inspection Data
Date: ___.:.\ l__;{c....:_! L=-{1..--'l~"J-l'itol Tube Identification: __ ...!.\_~:::__·-_:G:..· -------
Technician: __ ..:..M_:_:...• :._M.----":._~=-:....'".:.L::::o...:.;M_..:.:::.I.J...:::;(...:lA::..· ::._ _____ _
Dt=_·~3:....'"t'-'):._'_· __ in.
. '-1~<..
Is l',.. = P11 ? ~ €. S
Is 1.05 • D, $ D, s 1.50 • D, ?~~-'-y;....::-c-·:)L-~~~~~~~~=
p "' •
-'-lCCl.. ..:.l:"'s_"' ________ in.
<<t <Ill"
n2 < I o•
[1, < 5"
o, = ___ .:..._ __
":= _____ _
fit =---=2.=----
f\2= ___ 2 __ _
Z~O.t2S in . Z = _ _:•_:o~o~l ___ in.
. -~· ~~~.-~~-w
--j..:.;...:..--lf-1. ---·····---.. \~ ..
["u h -·~·••· '9-,--_,_
G:IJ I
£ t: ,, •• ,..... :::rJ::)
W ~ 0.03125 in.
W > 3 mchcs
Z > 3/4 itlCh
W= . oo e in
w,; (.. .)-in
Z= I' 10.
.~ ~~.Jd:~ 1-..... ---Y 2:3 inches Y = __ 3_,_)_,... __ n.
The pitottube m~cts the specifications for a calihmtion factor of0.84? '/-e. ~
Tcmp~mturc Scn~or Calibration
Ref,•rcncc·
·:<7~.~ Temperature Tcn\iicml!lle Temperature . ~ Source Rcfc.rencc Sensor Di~~nce J • ,, '•'~
o ••• ~ ... I ,• {Mediuml ("Fl ("PJ
AIR (2.. 1'2-0
Probe Continuity 'fe..S
Heat Check 248 'i-c..S l ro
AIR 11.. l'l.. 0
ICE WATER 3> 1y I
Stack BOIL WATER 21)'L 2oL 0
SILICONE OIL
TypeS Pilot Tube lnspt~ction Dala
Dat~: l2-13 ~-r.~ Pilot Tube ltl~-lltiliratim>: __ ...;'1=' :...-~~!-._-_(,.:=__ ____ _
Dt= .-y~) in Is P A= Pn? j~~
Ts 1.05 • D1 $ D1 $ 1.50·01 '? 'i~~
P, = ·i51. 10,
l'u = . ~12.. in.
C<t < 10° 0 .. Cl1 =
(.(2 < 101' (ll'=-0
11 , < s" 1\,~
fi,<S• j\,~
Z:<: 0 125 in. Z= .oiC, in
W s O.DJI25 in. W= •ooB in
W=
..,. _in.
l=
_J.!i::.:-1. W > :l inches '""'"'~" -~~-· F=· -~;;=w--Z>3/4inch
crwm '
Y = _3=-.;.'....:(:..._ __ in.
The pit0t tu~c meets tltc srll'ciftcations tor a calibration factor ofO R4?
Tcmpt'raturc Sensor Calibration
Reference· . .. ' Tempemlur¢ 'rcmpei3lurc Tc;nlfl<ltnlutl!
.,A • ~: :;11 ,1 Source Reference Sensor nirr(,~l\('
I (Medium) ('1') ("f) rn
AIR C..B (.,~ 1-
Probe Continuitv '/es
Heat Chcr.k 2·18 250 'ie5
AIR (o0 "Co 1
ICE WATER ~3 3'2. \
Stack [lOlL WATER l.ol{ 2o3 l
SILICONE OIL
TETCO
Sample Box Temperature Sensor Calibrution
Dote: 12/13/13 Calibmtor: Dean Kitchen Reference: Ome~aCL3512A
Thermocouple Temperature TC:OlflCf111Urc Temperature
l lnit 10 Location Sou•·ce Reference Sensor Difference
(Medium) t"F) ("F) !"F)
Oven Water 32 34 2
Water 204 203 -I
A Water 33 34 I Oven (4) Water 204 202 -2
lmpinger Out Water 33 34 I
Water 204 203 -I
Oven Water 33 33 0
Water 204 202 -2
B Oven (4) Watct· 33 34 I
Water 203 203 0
lmpinger Out Water 32 33 I
Water 204 202 -2
Oven Water 32 33 I
Water 204 203 -I
c Oven (4) Water 33 34 I
Water 204 204 ()
Water 33 '' () lmpinger Out .).)
Water 203 202 -I
Oven Water 33 34 I
Water 203 203 0
D Oven (4) Water 33 34 .1
Water 204 204 0
Water 33 '' 0 lmpinger Out .>.)
Water 204 202 -2
Oven Water 33 34 I
Water 203 202 -I
E Oven(4) Water 33 33 0
Water 204 203 -I I
lmpinger Out Water 33 34 1
Water 204 203 -1
Oven Water 33 34 I
Water 204 202 -2
F Oven (4) Water 33 34 1
Water 204 202 -2
lmpinger Out Water 33 33 0
Water 203 202 ·I
lmpinger Out G Water 33 34 I
Water 204 203 -I
;-Water 33 34 I lrnpingcr Out H Water 204 202 -2
lmpinger Out I Water 33 33 ()
Water 204 202 -2
lmpinger Out J Water 33 34 I
Water 203 202 -I
APPENDIXF
The testing followed the same procedures as outlined in previous protocols and tests at this
facility.
ATTACHMENT H
SURFACE WATER GRAPHS AND FIELD DATA SHEETS
1.00E-05
1.00E-06
1.00E-07
-~
C'CI ~.OOE-08
m 0 ...J -
1.00E-09
._ ....
.... ·-
---...
.... ....
• -
... --;;. ----
1.00E-10 ---
1.00E-11
9:>~
\..._OJ ~"'
~ -:..to..Oj ~~
Cottonwood Creek Dissolved Radionuclide Concentrations
(uCi/ml)
-
-
... •
• -
---.. • ..... .. -
I
o_,OJ~ ~"
.... ~"'
--.....
•
• ~
..
-
• ....
~ • • --
-. • ... .... ...........
?.>co ~ .... Oj ~(c)
~~ ~ ~ to.."'
I • U-N at. • Th-230 • R-;-226]
~OJ ~ <d-..._OJ
...
-
4
--
.. •
~·
--
..._b<
f.}<f>
to.."'
~ <d-~tf>
Cottonwood Creek Suspended Radionuclide Concentrations (uCi/ml)
1.00E-06 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
•
1.00E-07 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ . ---• -
1.aoE-oa l • • • •] : •• : • • I ... • i ---. .. .. , = •
..... . • • a - --.._.. ---. ..._ ...._ ----------------------------..------......_____ .... -·----. --~------------------__ _..._......______ -......-------. -
1.00E-10 • .&
1.00E-11 !~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
1.00E-12 , , ,
~(,;)
':-."q) ~"'
~ ~"q) cy.~
B~ ~"Oj
rd-rf'
Bn;, ~"Oj ~~
~ .__OJOJ ~ .__tV
B<o ~"Oj cy."f;;j
~"
rd-rd-fS
~~ ~rVrv
~co ~ ~ ""'
j • U-Nat. • Th-230 & Ra-226]
~Oj ~ q}~
~.__'1, cy.rv
~"
~ ~ rV"Oj
~~ ~rv
""'
Westwater Creek Suspended Radionuclide Concentrations (uCi/ml)
1 ~~~~~~~~~~~~~
0.1 ~~~~~~~~~~~~~~~~~~~~~~~~
0.01 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
0.001
0.0001 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
0.00001
~ ~.000001 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
~000001 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1E-08 iiii~~~~~ii~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1 E-og l·iiii~ii:iii!;~~~~~~~ii~~!!~!!~!!~~!::!~!!!:~!i~ii~~~iiiii 1E-10 •
1 E-11
1E-12 ~~~~~~~~~~~iiii~~~~~~~~~~~~~~~~~~~~~~~~~~~~! 1E-13 , .
§>OJ /t,:~ ~..__r;;:, ~~f)) ~..__r;;:, ~..__~
~..__..__
~~
..__
~..__
cy.~
,..__~
~to.;.
I • U-Nat • Th 230 & Ra-226 ]
~..__~ ~..__co ..__~
~..__":> ~ro
,..__":>
~f))
..__..-.
0.1
0.01
0.001
0.0001
0.00001 -Cl)
1jl.000001 en
tJ)
~0000001 -
1E-08
1E-09
1 E-10
1 E-11
1 E-12
1 E-13
r::;,~Oj
~,~~
-
...... ~ ~ ~'),rv
Westwater Creek Dissolved Radionuclide Concentrations
(uCi/ml)
...... ~ ~~ ~"r::s "" ~ ~~ "" ~ cy.~
~
r:::,"'-'1,
~~~
I • U-Nat. • Th-230 • Ra-226 I
r:::,"'-'1,
~~
...... rS-"
r:::,"~ ~~~
-
...
...... ~ ~ ~rv
""
EI\ERGY
• 1\ .. l:'")il/\T·~-::ntr':..l
www.energylab.com
AMJyt/I:M Ezullua .. 11/52
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-686-7175 • Rapid City, SD 888-&72-1225 • College Station, 1X 888-690-2218
January 30, 2014
Energy Fuels Resources (USA) Inc
225 Union Blvd Ste 600
Lakewood, CO 80228-1826
Workorder No.: C13090424
ANAL VTICAL SUMMARY REPORT
Project Name: 3rd Quarter Surtace Water 2013 Resample
Energy Laboratories, Inc. Casper WY received the following 4 samples for Energy Fuels Resources (USA) Inc on 9/12/2013
for analysis.
Sample ID Client Sample ID Collect Date Receive Date Matrix Test
C13090424-001 Cottonwood Creek 09/1 0/13 12:15 09/12/13
C13090424-002 Cottonwood 65 09/1 0/13 12:15 09/12/13
C 13090424-003 Westwater Canyon 09/1 0/13 12:35 09/12/13
Aqueous
Aqueous
Aqueous
Solids, Total Dissolved
Solids, Total Suspended
Same As Above
Sample Filtering
Uranium, Dissolved
Uranium, Suspended
Digestion, Total Metals
Gross Alpha, Gross Beta
Radium 226, Dissolved
Radium 226, Suspended
Thorium, Isotopic
Thorium, Suspended Isotopic
Solids, Total Dissolved
Solids, Total Suspended
C13090424-004 Temp Blank 09/12/13 Aqueous Temperature
The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were
pertormed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted.
Radiochemistry analyses were pertormed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601,
unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical
Report, the QA/QC Summary Report, or the Case Narrative.
If you have any questions regarding these test results, please call.
Report Approved By:
c)~£) tJrj_~
Reporting Supervisor
Digitally signed by
Stephanie Waldrop
Date: 2014.01.30 12:20:08 -07:00
Page 1 of 14
EN:RGY
*~,,~=....,.J li\ I { li <I· '
www.energylab.com
~~S/Dul/152
Helena, MT 877-472-0711 • Billings, MT 808-735-4489 • Casper, WY 888-235-0515
Gillette, WY 86&-68&-7175 • Rapid City, SO 888-612-1225 • College Station, TX 888-690-2218
CLIENT: Energy Fuels Resources (USA) Inc
Project: 3rd Quarter Surface Water 2013 Resample
Sample Delivery Group: C13090424
TDS ANALYSIS COMMENTS
Revised Date: 01/30/14
Report Date: 10/10/13
CASE NARRATIVE
The TDS result for sample -003 (Westwater Canyon) was analyzed past the recommended hold time due to reanalysis. The
original analysis was done within hold, however, due to sample matrix effects, insufficient volume was used causing an
increased reporting limit. This original analysis was done on 9/13/13 with a result of ND at an RL of 200. The sample was
reanalyzed 6 more times in an effort to achieve a result above the RL. Unfortunatelty, when a reportable result was achieved
the holding time had already expired. Despite the analysis being past hold time, the laboratory is confident in the result and has
duplicate analysis to support the reported result (230 mg/L, 317 mg/L, 205 mg/L).
REVISED/SUPPLEMENTAL REPORT
The attached analytical report has been revised from a previously submitted report due to the request by Kathy Weinel on
January 30, 2014 to add an explanation concerning the TDS analysis on sample -003. The report has been revised and
replaces any previously issued report in its entirety.
ORIGINAL SAMPLE SUBMITIAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4'C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this
method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should
be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of
counting should not exceed 8 days.
SOIUSOliD SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB
monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b-Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r-Energy Laboratories, Inc. -Rapid City, SD
eli-cs-Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under
these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of
origin. Please verify Ell's certification coverage by visiting www.energylab.com
Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web
page www.energylab.com.
Page 2 of 14
EI\ERGY
_ '\ljO•t/ I (JHI -·~
www.energylab.com
AM~ybl~Shms tiiU
Helena, MT 877-472-0711 • Billings, MT BGD-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&8-&86-7115 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 01/30/14
Report Date: 10/10/13
Collection Date: 09/10/13 12:15
Date Received: 09/12/13
Matrix: Aqueous
Client: Energy Fuels Resources (USA) Inc
Project:
LabiD:
3rd Quarter Surface Water 2013 Resample
c 13090424-00 1
Client Sample ID: Cottonwood Creek
Analyses
PHYSICAL PROPERTIES
Solids, Total Dissolved TDS@ 180 C
Solids, Total Suspended TSS@ 105 C
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
320 mgll
16500 mgll
D -RL increased due to sample matrix.
MCLI
Qualifiers RL QCL Method Analysis Date 1 By
200 A2540 C 09116113 14:26 I tmm
D 300 A2540 D 0911311314:311tmm
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 3 of 14
www.energylab.com
AlulytkM~Sfla 1151
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 886-88&-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-&90-221 8
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 01/30/14
Report Date: 10/10/13
Collection Date: 09/10/13 12:15
DateReceived: 09/12/13
Matrix: Aqueous
Client: Energy Fuels Resources (USA) Inc
Project:
Lab ID:
3rd Quarter Surface Water 2013 Resample
c 13090424-002
Client Sample ID: Cottonwood 65
Analyses
PHYSICAL PROPERTIES
Solids, Total Dissolved TDS@ 180 C
Solids, Total Suspended TSS@ 105 C
Report
Definitions:
RL -Analyte reporting limit.
QCL-Quality control limit.
Result Units
300 mg/L
21800 mg/L
D -RL increased due to sample matrix.
MCLI
Qualifiers RL QCL Method Analysis Date I By
200 A2540 C 09/16/13 14:26/tmm
D 300 A2540 D 09/13/13 14:31/tmm
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 4 of 14
EN:RGY
1\HC~I\f•";':Pi f ·_;
MNW.energylab.com
AJgfytlai~Sinu rm
Helena, MT 177-472-0711 • Billings, MT BOI-735-4489 • Casper, WY 888-235-0515
Glllatta, WY 866-688-7175 • Rapid City, SD 888-172-1225 • College Station, 1X 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch Revised Date: 01/30/14
Report Date: 10/10/13
Collection Date: 09/10/13 12:35
Date Received: 09/12/13
Matrix: Aqueous
Client: Energy Fuels Resources (USA) Inc
Project:
Lab ID:
3rd Quarter Surface Water 2013 Resample
c 13090424-003
Client Sample ID: Westwater Canyon
Analyses
PHYSICAL PROPERTIES
Solids, Total Dissolved TDS@ 180 C
Solids, Total Suspended TSS@ 105 C
-See Case Narrative for TDS analysis comments.
METALS -DISSOLVED
Uranium
METALS-SUSPENDED
Uranium
RADIONUCLIDES-DISSOLVED
Gross Alpha
Gross Alpha precision (±)
Gross Alpha MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
RADIONUCLIDES -SUSPENDED
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL-Quality control limit.
Result Units
260 mgiL
16700 mgiL
0.0108 mgiL
0.0176 mgll
20.4 pCiiL
1.9 pCiiL
2.0 pCiiL
0.68 pCiiL
0.19 pCiiL
0.19 pCiiL
0.2 pCiiL
0.1 pCiiL
0.2 pCiiL
28 pCiiL
1.2 pCiiL
0.21 pCiiL
8.7 pCiiL
2.2 pCiiL
1.1 pCiiL
MDC -Minimum detectable concentration
Qualifiers
H
D
D
H -Analysis performed past recommended holding time.
MCU
Rl QCL Method Analysis Date I By
200 A2540 C 09117113 14:56 I alp
300 A2540 D 0911311314:311tmm
0.0003 E200.8 09116113 17:38 I elm
0.0009 E200.8 09120113 15:58 I elm
E900.0 09119113 18:19 11bb
E900.0 09119113 18:19 llbb
E900.0 09119113 18:19 llbb
E903.0 0913011318:5711mc
E903.0 0913011318:5711mc
E903.0 09130113 18:57 lime
E908.0 09119113 17:17 I dmf
E908.0 09119113 17:17 I dmf
E908.0 09119113 17:17 I dmf
E903.0 09124113 23:36 I lmc
E903.0 09124113 23:3611mc
E903.0 09124113 23:36 I lmc
E908.0 09130113 09:09 I dmf
E908.0 09130113 09:09 I dmf
E908.0 09130113 09:09 I dmf
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 5 of 14
EN:RGY
ASCR~·~a cH--I•L:::O
Client:
Project:
LabiD:
.· ~~~WW.energylab.com
~~S/((C# fiSt
Helena, MT 877-472-0711 • BillinKs, MT BOD-735-4489 • Casper, WY 888-235-0515
Gillette, WY 888-888-7175 • Rapid City, SD 888-112-1225 • CGIIege Station, 1X 888-690-2218
LABORATORY ANAL VTICAL REPORT
Prepared by Casper, WY Branch
Energy Fuels Resources (USA) Inc
3rd Quarter Surface Water 2013 Resample
c 13090424-004
Client Sample ID: Temp Blank
Revised Date: 01/30/14
Report Date: 10/10/13
Collection Date: Not Provided
DateReceived: 09/12/13
Matrix: Aqueous
Analyses
PHYSICAL PROPERTIES
Temperature
Report
Definitions:
RL -Analyte reporting limit.
QCL-Quality control limit.
Result Units Qualifiers
3.4 "C
MCL/
RL QCL Method Analysis Date I By
E170.1 09112113 12:30 I kbh
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 6 of 14
EI\ERGY
_1\.~on~"' CIJif.-~
www.energyfab.com
bMyflal Exallwa Slta 11152
Helena, MT 877-472-0711 • Billings, MT BGD-735-4489 • Casper, WY 888-235·0515
Gillette, WY 8&6-186-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 01/30/14
Report Date: 10/10/13
Work Order: C13090424
Client: Energy Fuels Resources (USA) Inc
Project: 3rd Quarter Surface Water 2013 Resample
Analyte Count Result Units
Method: A2540C
SampleiD: MB-1_130916A Method Blank
Solids, Total Dissolved TDS@ 180 C NO mg/L
Sample ID: LCS·2_130916A Laboratory Control Sample
Solids, Total Dissolved TDS@ 180 C 1980 mg/L
Sample ID: C13090418·013A DUP Sample Duplicate
Solids, Total Dissolved TDS@ 180 C 41400 mg/L
Sample ID: C13090498·001A MS Sample Matrix Spike
Solids, Total Dissolved TDS@ 180 C 48400 mg/L
Method: A2540 c
Sample ID: MB-1_130917A Method Blank
Solids, Total Dissolved TDS@ 180 C NO mg/L
Sample ID: LCS-2_130917A Laboratory Control Sample
Solids, Total Dissolved TDS@ 180 C 1980 mg/L
Sample ID: C13090424-001A DUP Sample Duplicate
Solids, Total Dissolved TDS @ 180 C 340 mg/L
Sample ID: C13090504-001B MS Sample Matrix Spike
Solids, Total Dissolved TDS@ 180 C 2210 mg/L
Qualifiers:
RL-Analyte reporting limit.
MDC-Minimum detectable concentration
RL %REC Low Limit High Limit RPD RPDLimit Qual
Batch: TDS130916A
Run: BAL-19_130916B 09/16/13 14:24
10
Run: BAL-19_130916B 09/16/13 14:24
20 99 90 110
Run: BAL-19_1309168 09/16/1314:25
500 1.9 5
Run: BAL-19_130916B 09/16/13 14:27
200 103 90 110
Batch: TDS130917A
Run: BAL-19_130917A 09/17/13 14:53
10
Run: BAL-19_130917A 09/17/13 14:54
20 99 90 110
Run: BAL-19_130917A 09/17/13 14:54
200 0.0 5
Run: BAL-19_130917A 09/17/13 14:58
11 100 90 110
NO-Not detected at the reporting limit.
Page 7 of 14
EI\ERGY
. f\lHJf.:J\"1 OHir-::,
1'1 w.vw.energylab.com
AM/yflai~S.C. 11152
Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Glllatta, WY 816-186-7175 • Rapid City, SD 188-672-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 01/30/14
Report Date: 10/10/13
Work Order: C13090424
Client: Energy Fuels Resources (USA) Inc
Project: 3rd Quarter Surface Water 2013 Resample
Analyte Count Result Units
Method: A2540 0
Sample 10: MBLK1_130913 Method Blank
Solids, Total Suspended TSS @ 105 C NO mg/L
Sample 10: LCS1_130913 Laboratory Control Sample
Solids, Total Suspended TSS @ 105 C 199 mg/L
Sample 10: C13090508-003AOUP Sample Duplicate
Solids, Total Suspended TSS@ 105 C NO mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit
Run: BAL-19_1309138
2
Run: BAL-19_1309138
10 99 80 120
Run: BAL-19_1309138
10
NO-Not detected at the reporting limit.
RPO RPOLimit Qual
Batch: 130913_1_SLDS-TSS-W
09/13/1314:28
09/13/13 14:29
09/13/13 14:33
5
Page 8 of 14
EI\ERGY
1\;.)(JJU\.1 UH I~_·;
www.energylab.com
AMiytlal &c.llwru SiRu IW
Helena, MT 877-472-0711 • Billings, MT BOO-J:J5-4489 • Casper, WY 888-235-0515
Gillette, WY 866-&86-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 01/30/14
Report Date: 10/10/13
Work Order: C13090424
Client: Energy Fuels Resources (USA) Inc
Project: 3rd Quarter Surface Water 2013 Resample
Analyte Count Result Units RL
Method: E200.8
Sample 10: ICV Initial Calibration Verification Standard
Uranium 0.0517 mg/L 0.00030
Method: E200.8
Sample 10: LRB Method Blank
Uranium NO mg/L 1E-05
Sample 10: LFB Laboratory Fortified Blank
Uranium 0.0528 mg/L 0.00030
Sample 10: C13090332-003BMS4 Sample Matrix Spike
Uranium 0.0596 mg/L 0.00030
SampleiO: C13090332-003BMS04 Sample Matrix Spike Duplicate
Uranium 0.0592 mg/L 0.00030
Method: E200.8
Sample 10: ICV Initial Calibration Verification Standard
Uranium 0.0515 mg/L 0.00030
Method: E200.8
Sample 10~ MB-39040 Method Blank
Uranium NO mg/L 6E-05
Sample 10: LCS2-39040 Laboratory Control Sample
Uranium 0.0569 mg/L 0.00030
SampleiO: C13090424-0030MS Sample Matrix Spike
Uranium 0.771 mg/L 0.00090
Sample 10: C13090424-0030MSO Sample Matrix Spike Duplicate
Uranium 0.771 mg/L 0.00090
Qualifiers:
%REC Low Limit High Limit RPO RPOLimit Qual
Analytical Run: ICPMS2-C_130916A
09/16/13 14:40
103 90 110
Batch: R178350
Run: ICPMS2-C_130916A 09/16/13 15:06
Run: ICPMS2-C_130916A 09/16/1315:09
106 85 115
Run: ICPMS2-C_130916A 09/16/13 19:02
119 70 130
Run: ICPMS2-C_130916A 09/16/13 19:05
118 70 130 0.7 20
Analytical Run: ICPMS2-C_130920A
09/20/13 22:41
103 90 110
Batch: 39040
Run: ICPMS2-C_130920A 09/20/13 15:36
Run: ICPMS2-C_130920A 09/20/13 15:39
114 85 115
Run: ICPMS2-C_130920A 09/20/13 1 6 :09
97 70 130
Run: ICPMS2-C_130920A 09/20/13 16:12
97 70 130 0.1 20
RL-Analyte reporting limit. NO -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 9 of 14
EI\ERGY
._1\e!O !lAI C''f.41:...._5
www.ellef&Yiab.com
AJI/ytfQI~SfltU 1952
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 81&-186-7175 • Rapid City, SD 888-872-1225 • College Station, TX 888-690-2218
QAJQC Summary Report
Prepared by Casper, WY Branch Revised Date: 01/30/14
Report Date: 1 0/1 0/13
Work Order: C13090424
Client: Energy Fuels Resources (USA) Inc
Project: 3rd Quarter Surface Water 2013 Resample
Analyte
Method: E900.0
Sample 10: Th23G-GrAB-1623
Gross Alpha
Sample ID: MB-GrAB-1623
Gross Alpha
Gross Alpha precision (±)
Gross Alpha MDC
Sample ID: C13090424-003CMS
Gross Alpha
Sample ID: C13090424-003CMSD
Gross Alpha
Sample 10: C13090472-001EDUP
Gross Alpha
Gross Alpha precision (±)
Gross Alpha MDC
Qualifiers:
RL-Analyte reporting limit.
Count Result Units
Laboratory Control Sample
124 pCi/L
3 Method Blank
1 pCi/L
0.7 pCi/L
pCi/L
Sample Matrix Spike
142 pCi/L
Sample Matrix Spike Duplicate
129 pCi/L
3 Sample Duplicate
27800 pCi/L
65.7 pCi/L
3.12 pCi/L
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit
Run: G542M_130918A
117 80 120
Run: G542M_130918A
Run: G542M_130918A
115 70 130
Run: G542M_130918A
103 70 130
Run: G542M_130918A
ND -Not detected at the reporting limit.
RPD RPDLimit Qual
9.3
7.6
Batch: GrAB-1623
09/19/13 18:19
09/19/13 18:19
u
09/19/1318:19
09/19/1318:19
16
09/20/13 08:08
10.5
U -Not detected at minimum detectable concentration
Page 10 of 14
EN:RGY
A tt'-•LAr uJtll :..>
www.energylab.com
~~S.C.III51
Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-8515
Gillette, WY 816-18&-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218
QAIQC Summary Report
Prepared by Casper, WY Branch Revised Date: 01/30/14
Report Date: 10/10/13
Work Order: C13090424
Client: Energy Fuels Resources (USA) Inc
Project: 3rd Quarter Surface Water 2013 Resample
Analyte Count Result Units
Method: E903.0
Sample ID: C13090424-003DDUP 3 Sample Duplicate
Radium 226 25 pCi/L
Radium 226 precision (±)
Radium 226 MDC
Sample ID: C13090472-001HMS
Radium 226
1.1
0.20
pCi/L
pCi/L
Sample Matrix Spike
16 pCi/L
RL %REC Low Limit High Limit RPD RPDLimlt Qual
Run: BERTHOLD 770-1_130918B
11
Run: BERTHOLD 770-1_130918B
60 70 130
Batch: 39040
09/24/13 23:36
18.9
09/24/13 23:36
s
-Spike response is outside of the acceptance range for this analysis. Since the LCS and the RPD for the Duplicate are acceptable the batch is approved.
Sample ID: LCS-39040
Radium 226
Sample ID: MB-39040
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Method: E903.0
Sample ID: C13090702-001CMS
Radium 226
Sample ID: C13090702-001CMSD
Radium 226
Sample ID: MB-RA226-6857
Radium226
Radium 226 precision (±)
Radium 226 MDC
Sample ID: LCS-RA226-6857
Radium 226
Qualifiers:
RL -Analyte reporting limit.
Laboratory Control Sample
21 pCi/L
3 Method Blank
0.1
0.2
0.3
pCi/L
pCi/L
pCi/L
Sample Matrix Spike
40 pCi/L
Sample Matrix Spike Duplicate
41 pCi/L
3 Method Blank
0.002 pCi/L
0.06 pCi/L
0.1 pCi/L
Laboratory Control Sample
10 pCi/L
MDC -Minimum detectable concentration
U-Nol detected at minimum detectable concentration
Run: BERTHOLD 770-1_130918B
97 80 120
Run: BERTHOLD 770-1_130918B
Run: BERTHOLD 770-2_130924A
87 70 130
Run: BERTHOLD 770-2_130924A
89 70 130 2.2
Run: BERTHOLD 770-2_130924A
Run: BERTHOLD 770-2_130924A
92 80 120
NO -Not detected at the reporting limit.
S-Spike recovery outside of advisory limits.
09/24/13 23:36
09/24/13 23:36
u
Batch: RA226-6857
09/30/13 15:23
09/30/13 15:23
18.8
09/30/1318:57
u
09/30/13 18:57
Page 11 of 14
EI'ERGY
.• /'\HCH•/~J(.,f:411 '-·
www.energylab.com
AllfTtkal ~~5/nu IW
Helena, MT 877-472-0711 • Billings, MT BG0-735-4489 • Casper, WY 888-235-0515
Gillatta, WY 81&-186-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch Revised Date: 01/30/14
Report Date: 1 0/1 0/13
Work Order: C13090424
Client: Energy Fuels Resources (USA) Inc
Project: 3rd Quarter Surface Water 2013 Resample
Analyte
Method: E908.0
Sample ID: LCS-RA-TH-IS0-1911
Thorium 230
Sample ID: C13090078-003EMS
Thorium 230
Sample ID: C13090078-003EMSD
Thorium 230
Sample ID: MB-RA-TH-IS0-1911
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Method: E908.0
Sample ID: MB-39040
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Sample ID: LCS-39040
Thorium 230
Sample ID: C13090765-001CMS
Thorium 230
Sample ID: C13090765-001CMSD
Thorium 230
Qualifiers:
RL • Analyte reporting limit.
Count Result Units
Laboratory Control Sample
5.7 pCi/L
Sample Matrix Spike
13 pCi/L
Sample Matrix Spike Duplicate
13 pCi/L
3 Method Blank
0.1 pCi/L
0.1 pCi/L
0.2 pCi/L
3 Method Blank
0.5 pCi/L
0.4 pCi/L
0.5 pCi/L
Laboratory Control Sample
19 pCi/L
Sample Matrix Spike
12 pCi/L
Sample Matrix Spike Duplicate
11 pCi/L
MDC -Minimum detectable concentration
RL o/cfiEC Low Limit High Limit RPD RPDLimlt Qual
Batch: RA-TH-IS0-1911
Run: ALPHANALYST_130917A
87 80 120
Run: ALPHANALYST_130917A
99 70 130
Run: ALPHANALYST_130917A
99 70 130 0.1
Run: ALPHANALYST _130917A
Run: ALPHANAL YST _130925A
Run: ALPHANAL YST_130925A
103 80 120
Run: ALPHANALYST_130925A
100 70 130
Run: ALPHANAL YST_130925A
96 70 130 4.6
NO-Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
09/19/13 17:17
09/19/13 17:17
09/19/13 17:17
41.5
09/19/13 17:17
u
Batch: R178953
09/30/13 09 :09
u
09/30/13 09:09
09/30/13 09:09
09/30/13 09 :09
42.4
Page 12 of 14
EI\ERGY
." ... •-IIJ!··~ I •".f .. l :._
www.energylab.com
Aivllllul~ll-smu rm
Helena, MT 877-472-0711 • Billings, MT BOD-735-4489 • Casper, WY 888-235-0515
Gillette, WY BBB-888-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218
Workorder Receipt Checklist
Energy Fuels Resources (USA) Inc
Login completed by: Corinne Wagner
Reviewed by:
Reviewed Date:
Kathy Hamre
9/13/2013
Shipping container/cooler in good condition?
Custody seals intact on all shipping container(s)/cooler(s)?
Custody seals intact on all sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
(Exclude analyses that are considered field parameters
such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.)
Temp Blank received in all shipping container(s)/cooler(s)?
Container/Temp Blank temperature:
Water -VOA vials have zero headspace?
Water -pH acceptable upon receipt?
Yes 0
Yes 0
Yes D
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
3.4"C
Yes D
Yes 0
C13090424
Date Received: 9/12/2013
Received by: cav
Carrier Ground
name:
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
Not Present D
Not Present D
Not Present 0
Not Applicable D
No VOA vials submitted 0
Not Applicable D
=-----==------=====--=---=---=------==-=-=--===---==::-;:::::::=::.=::.-______ :..-:::::-.:::::-.:::::::_-_-_-::_-_-_-_-_-___ -_-_-_-_-_. __ _
Standard Reporting Procedures:
Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as
pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time.
Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected,
data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried
and ground prior to sample analysis.
Contact and Corrective Action Comments:
None
Page 13 of 14
1· Sheet 1 of 1
!!! .. .....·.~ """"'·~' ...._·
CHAIN OF CUSTODY
Samples Shipped to: -:E:::n=:er='"g~y...;;;L~ab:;o;:.;.ra;;;;;t~o::.:.;rie:..:s;__ _____ Contact: Garrin Palmer
2393 Salt Creek Hwy Ph: 435 678 2108
Casper WY, 82601 [e-mail]
Chain of Custody/Sampling Analysis Request
p . roJect
3rd Quarter Surface Water
2013 Re Sample
Date
Sample ID Collected
Cottonwood Creek 9/10/2013
Cottonwood 65 9/10/2013
Westwater Canyon 9/10/2013
Comments:
Relinquished By:(Signature)
s amp1ers N a me s amp1ers Sl tu 1gna r:e
Garrin Palmer G~ p~
Time
Collected Laboratory Analysis Requested
1215 Total Dissolved Solids, Total Suspended Solids
1215 Total Dissolved Solids, Total Suspended Solids
1235 Total Dissolved Solids, Total Suspended Solids
Grosh Alpha
Suspended U-nat,Dissolved U-nat
Suspended Ra-226, Dissolved Ra-226
Suspended Th-230, Dissolved Th-230
Samples were NOT field filtered orpJeserved.
.-.1!!...--r. J); I "" \c.. s. I { J. "-.}
' ~
Date/Time Received By:(Signature) Date/Time
9/11/2013
1300
Date/Time
Page 14 of 14
Ef'.ER www.energylab.com Helena, liT 817-472-0711 • Blllinp, liT U-731-4481 • Ca•per, WY 111-23&-1111 .,Eiclllla,_ tilt Gilletle, WY 118-118-7171 • Rapl,d City, SD 818-172-1221 • CGileteStatiOII, TX 111-110-2218
December 20, 2013
Energy Fuels Resources (USA) Inc
225 Union Blvd Ste 600
Lakewood, CO 80228-1826
WorkorderNo.: C13111072
ANALYTICAL SUMMARY REPORT
Project Name: 4th Quarter Surface Water 2013
Energy Laboratories, Inc. Casper WY received the following 1 sample for Energy Fuels Resources (USA) Inc on 11/27/2013
for analysis.
Sample ID Client Sample ID
C 13111 072-001 Cottonwood Creek
Collect Date Receive Date Matrix Test
11/25/13 12:25 11/27/13 Surface Water Sample Filtering
Uranium, Dissolved
Uranium, Suspended
Digestion, Total Metals
Gross Alpha, Gross Beta
Radium 226, Dissolved
Radium 226, Suspended
Thorium, Isotopic
Thorium, Suspended Isotopic
Solids, Total Dissolved
Solids, Total Suspended
The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were
performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted.
Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601,
unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical
Report, the QA/QC Summary Report, or the Case Narrative.
If you have any questions regarding these test results, please call.
Report Approved By: Digitally signed by
Sheri M. Mead
Date: 2013.12.20 13:34:55 -07:00
Page 1 of 11
EN:RGY
I ' ' '
Helena, MT 877-472-11711 • Bllllnlt, MT 101·135-4411 • Casper, WY III-23H515
Gllllttll, WY 111-181·7175 • Rapid City, SD 111-172·1225 • Colleae Station, lllll-&18-2211
CLIENT: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Surface Water 2013 Report Date: 12/20/13
Sample Delivery Group: C13111 072 CASE NARRATIVE
ORIGINAL SAMPLE SUBMITIAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand
delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this
method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should
be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of
counting should not exceed B days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven
individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB
monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its
branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b-Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r-Energy Laboratories, Inc. -Rapid City, SD
eli-cs -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
US EPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641 , Radiochemical E871 017; California: 02118CA;
Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under
these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of
origin. Please verify Ell's certification coverage by visiting www.energylab.com
Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web
page www.energylab.com.
Page 2 of 11
EI\ERGY
..
/ ... ·I· ... I' 'I ••
www.energylab.com
Mll!f/ell~ .. ,.
Helena, MT 117-472-8711 • Blllinp, MT 801-735-4489 • Casper, WY 811-23&-1111
Gillette, WY 116-118-7115 • Rapid City, SD 118-172-1225 • College Station, 1X 811-&ID-2211
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Surface Water 2013
LabiD: C13111072-001
Client Sample ID: Cottonwood Creek
Analyses Result Units
PHYSICAL PROPERTIES
Solids, Total Dissolved TDS@ 180 C
Solids, Total Suspended TSS@ 105 C
METALS -DISSOLVED
Uranium
METALS-SUSPENDED
Uranium
RADIONUCLIDES-DISSOLVED
Gross Alpha
Gross Alpha precision (±)
Gross Alpha MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
RADIONUCLIDES -SUSPENDED
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
287
410
0.0084
0.0005
10.8
1.6
2.1
1.8
0.23
0.12
0.2
0.1
0.2
0.68
0.24
0.26
0.2
0.1
0.2
MDC -Minimum detectable concentration
mgll
mgll
mgll
mgll
pCiiL
pCiiL
pCiiL
pCiiL
pCiiL
pCiiL
pCi/L
pCiiL
pCiiL
pCiiL
pCiiL
pCiiL
pCiiL
pCiiL
pCi/L
Qualifiers
D
u
U -Not detected at minimum detectable concentration
RL
10
10
0.0003
0.0003
MCL/
Report Date: 12/20/13
Collection Date: 11/25/13 12:25
Date Received: 11/27/13
Matrix: Surface Water
QCL Method Analysis Date I By
A2540 C
A2540 D
E200.8
E200.8
E900.0
E900.0
E900.0
E903.0
E903.0
E903.0
E908.0
E908.0
E908.0
E903.0
E903.0
E903.0
E908.0
E908.0
E908.0
11127113 15:48 I tmm
11127113 12:40 I alp
12102113 17:59 I elm
12103113 22:58 I elm
12111113 07:43 I lbb
12111113 07:43 I lbb
12111113 07:43 I lbb
12116113 11 :46 I I me
12116113 11:46 I lmc
12116113 11:46 I lmc
12117113 09:49 I dmf
12117113 09:49 I dmf
12117113 09:49 I dmf
1211611310:12 I lmc
12116113 10:12 I I me
12116113 10:12 I I me
12117113 14:35 I dmf
12117113 14:35 I dmf
12117113 14:35 I dmf
MCL-Maximum contaminant level.
NO -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 3 of 11
Helena, MT 871-472-8711 • Blllinp, MT 801-735-4411 • Cuper, WY 811-235-1515
Glllatte, WY 116-188-7175 • Rapid City, SD 118-172-1225 • College Station, TX 811-110-2211
QAJQC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Surface Water 2013
Analyte Count Result
Method: A2540 c
Sample ID: MB·1_131127A Method Blank
Solids, Total Dissolved TDS@ 180 C ND
Units
mg/L
Sample ID: LCS-2_131127A Laboratory Control Sample
Solids, Total Dissolved TDS @ 180 C 2020 mg/L
Sample ID: C13111074-008A MS Sample Matrix Spike
Solids, Total Dissolved TDS@ 180 C 20900 mg/L
Sample ID: C13111079-006A DUP Sample Duplicate
Solids, Total Dissolved TDS@ 180 C 439 mg/L
Qualifiers:
RL-Analyte reporting limit.
MDC-Minimum detectable concentration
RL %REC
10
20 101
100 104
10
Report Date: 12/20/13
Work Order: C13111 072
Low Limit High Limit RPD RPDLimit Qual
Batch: TDS131127A
Run: BAL-19_131127B 11/27/1315:43
Run: BAL-19_1311278 11/27/13 15:43
90 110
Run: BAL-19_131127B 11/27/1315:53
90 110
Run: BAL-19_131127B 11/27/1315:57
1.4 5
ND-Not detected at the reporting limit.
Page 4 of 11
EI\ERGY
~ J: ,., ' ~' 'I
Heleaa, MT 817-472-11711 • Blllin&s, MT 101-735-44111 • Casper, WY 111-235-1515
Glllltta, WY 116-188-7171 • Rapid City, SD 118-172-1225 • Collaae Stati011, IX 811-110-2211
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Surface Water 2013
Analyte Count Result
Method: A2540 D
Sample ID: MBLK1_131127 Method Blank
Units
Solids, Total Suspended TSS@ 105 C NO mg/L
Sample ID: LCS1_131127 Laboratory Control Sample
Solids, Total Suspended TSS@ 105 C 191 mg/L
Sample ID: C13111027-001CDUP Sample Duplicate
Solids, Total Suspended TSS@ 105 C 74.0 mg/L
Qualifiers:
RL-Analyte reporting limit.
MDC-Minimum detectable concentration
Report Date: 12/20/13
Work Order: C13111 072
RL o/oREC Low Limit High Limit
Run: BAL-19_131127A
2
Run: BAL-19_131127A
10 95 BG 120
Run: BAL-19_131127A
12
NO-Not detected at the reporting limit.
RPD RPDLimit Qual
Batch: 131127_1_SLDS-TSS-W
11/27/13 12:37
11/27/13 12:38
11/27/13 12:38
5
Page 5 of 11
EI'ERGY
' •• j '\I 1• •
Heleaa, MT 8l7-472-G711 • Blllin&s, MT IGI-135-4419 • Caspllf, W'f 811-23~515
Gillatte, W'f 811-181-7175 • Rapid City, SD 118-172-1225 • College Stati011, IX 811-810-2211
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Surface Water 2013
Report Date: 12/20/13
Work Order: C13111 072
Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual
Method: E200.8 Analytical Run: ICPMS2·C_131202A
Sample ID: ICV Initial Calibration Verification Standard 12/02/13 17:24
Uranium 0.0477 mg/L 0.00030 95 90 110
Method: E200.8 Batch: R181375
Sample ID: LAB Method Blank Run: iCPMS2-C_131202A 12/02/13 15:06
Uranium NO mg/L 1E·05
Sample ID: LFB Laboratory Fortified Blank Run: ICPMS2-C_131202A 12/02/13 15:09
Uranium 0.0492 mg/L 0.00030 99 85 115
Sample ID: C13111 072-001 BMS Sample Matrix Spike Run: ICPMS2-C_131202A 12/02/13 1 8:02
Uranium 0.0624 mg/L 0.00030 108 70 130
SampleiD: C13111 072-001 BMSD Sample Matrix Spike Duplicate Run: ICPMS2-C_131202A 12/02/13 18:06
Uranium 0.0612 mg/L 0.00030 106 70 130 1.9 20
Method: E200.8 Analytical Run: ICPMS2-C _131203A
Sample ID: ICV Initial Calibration Verification Standard 12/03/13 19:37
Uranium 0.0473 mg/L 0.00030 95 90 110
Method: E200.8 Batch: 39923
Sample ID: MB-39923 Method Blank Run: ICPMS2-C_131203A 12/03/13 22:48
Uranium NO mg/L 0.0003
Sample ID: LCS2-39923 Laboratory Control Sample Run: ICPMS2-C_131203A 12/03/13 22:51
Uranium 0.0918 mg/L 0.00030 92 85 115
SampleiD: C13111 072-001DMS Sample Matrix Spike Run: ICPMS2-C_131203A 12/03/13 23:04
Uranium 0.0367 mg/L 0.00030 96 70 130
Sample ID: C13111 072-001 DMSD Sample Matrix Spike Duplicate Run: ICPMS2-C_131203A 12/03/13 23:08
Uranium 0.0371 mg/L 0.00030 96 70 130 0.9 20
Qualifiers:
RL-Analyte reporting limit. NO -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 6 of 11
EN:RGY
~ , • ~ F • • , ....., r • r • •
www.energylab.com
AMI1fal EzaiiMa Sit/a 11U
Helena, MT 877-472-0711 • Blllln11, MT 801-735-4411 • Casper, WY 811-235-1515
Gillatte, WY 118-188-7171 • Rapid City, SD 118-172-1225 • Collage Station, IX 811-&ID-2211
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Surface Water 2013
Analyte
Method: E900.0
Sample ID: Th230-GrAB-1671
Gross Alpha
Sample ID: MB-GrAB-1671
Gross Alpha
Gross Alpha precision (±)
Gross Alpha MDC
Count Result Units
Laboratory Control Sample
105 pCi/L
3 Method Blank
-1 pCi/L
0.7 pCi/L
pCi/L
Sample ID: C13111031-001FDUP 3 Sample Duplicate
Gross Alpha 2610 pCi/L
Gross Alpha precision (±)
Gross Alpha MDC
Sample ID: C13111072-001CMS
Gross Alpha
Sample ID: C13111072-001CMSD
Gross Alpha
Qualifiers:
RL-Analyte reporting limit.
MDC-Minimum detectable concentration
20.6 pCi/L
2.57 pCi/L
Sample Matrix Spike
108 pCi/L
Sample Matrix Spike Duplicate
110 pCi/L
Report Date: 12/20/13
Work Order: C 13111 072
RL %REC Low Limit High Limit
Run: G5000W_131209A
92 80 120
Run: G5000W_131209A
Run: G5000W_131209A
Run: G5000W_131209A
85 70 130
Run: G5000W_131209A
87 70 130
ND -Not detected at the reporting limit.
RPD RPDLimit Qual
3.3
2.2
Batch: GrAB-1671
12/10/1318:46
12/10/13 18:46
u
12/10/1318:46
11.6
12/11/13 07:43
12/11/13 07:43
16.2
U -Not detected at minimum detectable concentration
Page 7 of 11
EI'ERGY
,· 1'-.' ) • , ... , ~ ..... '
Helena, MT 871-472-0711 • Blllin1s, NT 801-735-441J9 • Casper, WY 811-235-1515
Glllatta, WY 118-IBI-7175 • Rapid City, SD 118-172-1225 • College Station, IX 811-tiD-2211
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Surface Water 2013
Report Date: 12/20/13
Work Order: C 13111 072
Analyte
Method: E903.0
Sample ID: C13120116-001GMS
Radium 226
Sample ID: C13120116-001GMSD
Radium 226
Sample ID: MB-RA226-6992
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Sample ID: LCS-RA226-6992
Radium 226
Method: E903.0
Sample ID: C13111072-001DMS
Radium 226
Sample ID: C13111072-001DMSD
Radium 226
Sample ID: LCS-39923
Radium 226
Sample ID: MB-39923
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Qualifiers:
RL -Analy1e reporting limit.
Count Result Units
Sample Matrix Spike
22 pCi/L
Sample Matrix Spike Duplicate
20 pCi/L
3 Method Blank
0.06 pCi/L
0.09 pCi/L
0.1 pCi/L
Laboratory Control Sample
11 pCi/L
Sample Matrix Spike
18 pCi/L
Sample Matrix Spike Duplicate
19 pCi/L
Laboratory Control Sample
24 pCi/L
3 Method Blank
-0.10 pCi/L
0.2 pCi/L
0.4 pCi/L
MDC -Minimum detectable concentration
RL %REC Low Limit High Limit
Run: G5000W_131209B
94 70 130
Run: G5000W_131209B
88 70 130
Run: G5000W_131209B
Run: G5000W_131209B
93 80 120
Run: G542M_131209A
106 70 130
Run: G542M_131209A
113 70 130
Run: G542M~131209A
113 80 120
Run: G542M_131209A
NO-Not detected at the reporting limit.
RPD RPDLimit Qual
6.3
6.1
Batch: RA226-6992
12/16/13 11:46
12/16/13 13:18
21.1
12/16/1313:18
u
12/16/13 13:18
Batch: 39923
12/16/13 10:12
12/16/1310:12
20.8
12/16/1310:12
12/16/1310:12
u
U -Not detected at minimum detectable concentration
Page 8 of 11
EI\ERGY
r., , I ' I • 1 ~''
www.energylab.com
~.~1Siei11S1 Helena, MT 877-472.0711 • Billings, MT 801-735-44811 • Casper, WY 888-235-1515
Gllllltte, WY 816-188-7175 • Rapid CitJ, SD 816-172-1225 • Collage Station, IX 888-810-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 4th Quarter Surface Water 2013
Analyte Count Result Units
Method: E908.0
Sample ID: LCS-RA-TH-IS0-1969
Thorium 230
Sample ID: C13111 072-001 CMS
Thorium 230
Sample ID: C13111072-001CMSD
Thorium 230
Sample ID: MB-RA-TH-IS0-1969
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Method: E908.0
Sample ID: C13111072-001DMS
Thorium 230
Sample ID: C13111072-001DMSD
Thorium 230
Sample ID: MB-39923
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Sample ID: LCS-39923
Thorium 230
Qualifiers:
RL-Analyte reporting limit.
3
3
MDC -Minimum detectable concentration
Laboratory Control Sample
6.6 pCi/L
Sample Matrix Spike
13 pCi/L
Sample Matrix Spike Duplicate
13 pCi/L
Method Blank
0.1 pCi/L
0.10 pCi/L
0.2 pCi/L
Sample Matrix Spike
14 pCi/L
Sample Matrix Spike Duplicate
15 pCi/L
Method Blank
0.3 pCi/L
0.3 pCi/L
0.5 pCi/L
Laboratory Control Sample
17 pCi/L
Report Date: 12/20/13
Work Order: C 13111 072
RL %REC Low Limit High Limit RPD RPDLimit Qual
Run: ALPHANALYST _131212B
99 80 120
Run: ALPHANALYST_131212B
97 70 130
Run: ALPHANALYST_131212B
102 70 130
Run: ALPHANALYST _131212B
Run: ALPHANAL YST _131212C
84 70 130
Run: ALPHANALYST _131212C
91 70 130
Run: ALPHANALYST_131212C
Run: ALPHANALYST_131212C
96 80 120
ND-Not detected at the reporting limit.
4.9
7.1
Batch: RA-TH-IS0-1969
12/17/13 09:48
12/17/13 09:49
12/17/13 09:49
45.6
12/17/13 09:49
u
Batch: 39923
12/17/13 14:35
12/17/13 14:35
39.9
12/17/13 14:35
u
12/17/13 14:35
U -Not detected at minimum detectable concentration
Page 9 of 11
EN:RGY
<' ' •
!Ill lena, MT 871-472-G711 • Blllinp, MT 101-735-4419 • Casper, W'f 111-235-1515
Gillette, W'f 118-188-7175 • Rapid Cit)', SD 111-172-1225 • Colleae Station, TX 811-&ID-2211
Workorder Receipt Checklist
Energy Fuels Resources (USA) Inc
Login completed by: Cori A. Velasquez
Reviewed by:
Reviewed Date:
BL2000\khelm
12/2/2013
Shipping container/cooler in good condition?
Custody seals intact on all shipping container(s)/cooler(s)?
Custody seals intact on all sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
(Exclude analyses that are considered field parameters
such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.)
Temp Blank received in all shipping container(s)/cooler(s)?
Container/Temp Blank temperature:
Water -VOA vials have zero headspace?
Water-pH acceptable upon receipt?
Yes 0
Yes 0
Yes D
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes D
1.6"C On Ice
Yes D
Yes 0
C13111072
Date Received: 11/27/2013
Received by: we
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
No 0
NoD
NoD
Carrier NDA
name:
Not Present D
Not Present D
Not Present 0
Not Applicable D
NoVOA vials submitted 0
Not Applicable 0
-------------------,------·---------------------------·---
Standard Reporting Procedures:
Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as
pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time.
Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected,
data units are typically noted as -<lry. For agricultural and mining soil parameters/characteristics, all samples are dried
and ground prior to sample analysis.
Contact and Corrective Action Comments:
None
Page 10 of 11
Sheet 1 of 1
CHAIN OF CUSTODY
Samples Shipped to: Energy Laboratories Contact: Garrin Palmer ..;2;::3==93~8-=a~lt ~C:=-;re~e~k:.:;H::=:wy=--------Ph: 435 678 4115
Casper WY, 82601 [e-mail]
Chain of Custody/Sampling Analysis Request
Proj~ct Samplers Name Samplers Signature
4th Quarter Surface Water {,.__;:;_ p~ 2013 Garrin Palmer
Time
SampleiD Date Collected Collected Laboratory Analysis ReQuested
CottonWood Creek 11/25/2013 1225 TDS
TSS
Dissolved Gross Alpha
Suspended U·nat
Dissolved U-nat
Suspended Ra-226
Dissolved Aa-226
Suspended Th-230
Dissolved Th-230
~ S...-tlu 6-.r... A/O"f" ~ii.J&rul .,r /JrL£.-r• .... L~
Comments: f"l.l'2..11• .,,,
'-' I I l J ' c;J""ooo
Relinquished By:(Signature) DatefTime Received By:(Sigmiture) Datemme
u~P~ ii/U~
lt.DO
Relinquished By:(Signature) Date/Time Received By:(Signature) D~~ ~ w"tk" c..--1'\ ''t u . :-r,
\. L )
Page 11 of 11
.·
' :··
White Mesa Mill-Standard Operating Procedures
Book #11 : Environmental Protection Manual, Section 2.1
Date: 2/07 Revision: DUSA-1
Page 5 of5
Attachment A
FIELD WATER ANALYSIS SURFACE WATER
WHITE MESA MILL
LOCATION (Circle one)tSi"onwoo.d Ci'~ We:;twater Canyon Other (describe) ____ _
{2. G.-$. t;.vv\. {) l "
DATE: 9 I I 0 ,, )
pH BUFFER 7.0 ( .. 0
BY: Ga. .... :""-&1...."'-('-C
(Sampler's initials)
pH BUFFER 4.0 __ '-l-=-=-=. D~---
SPECIFIC CONDUCTIVITY __ q_._.._q_.q _____ ---"u=M~H=O=s
STEAM DEPTH:
pHofWATER_~t~·-~~~~------------
'I
COND J.tmhos 1~0 COND j.tmhos l</0 .0
pH Units---='-'-~-"~----pH units __ ..::::!t~7....!........:l-IL__ __
Temp °C ---"'1...::6..:... -=-"'=D __ _
COND j.tmhos t"fD COND j.tmhos I t..to
pH units 6 .15 pH units $?. 7 3
Temp°C 16 gq
Comments:
.
.•
white Mesa Mill -Standard Operating Procedures Date: 2/07 Revision: DUSA-1
PageS of5 Book #11: Environmental Protection Manual, Section 2.1
Attachment A
FIELD WATER ANALYSIS SURFACE WATER
WHITE MESA MILL
LOCATION (Circle one):Cottonwood Creek Westwater Canyon Other (describe) ___ _
DATE: Cf J to {J3
pH BUFFER 7.0 __ ·7....., • ._,0oo<..,_ __ _
BY: 6c-r.r;~ P~l_.....,e..r
(Sampler's initials)
pH BUFFER 4.0 ----''1="-""0:;..,...._ __ _.
SPECIFIC CONDUCTIVITY _ _._9_.'f__.9 ______ _.u=M=H=O=s
STEAM DEPTH: l l'l.. Fl
pHofWATER r. 7'-/ TENW __ ~I~S~o-· c~·-~---
• I
CONDumhos 1'10 COND llill!lOS t'i 0. 3
pH Units ~.l~ pH units ~ .7'/
Temp°C lh C!D Temp °C _l_b_· .Cf...:...;D;__ __ __
COND !lmhos I~D COND !lmhos } ~ {)
pH units g:7S pH units 1£>.7 3
Temp°C i "· g 1 Temp °C ---'-i-=-t,__,g'o._j.__ __ _
Comments:
White Mesa Mill -Standard Operating Procedures
Book #11: Environmental Protection Manual, Section 2.1
Date: 2/07 Revision: DUSA-1
Page 5 of5
Attachment A
FIELD WATER ANALYSIS SURFACE WATER
WHITE MESA MILL
LOCATION (Circle one ):Cottonwood Creek (}[estwater Can~ Other (describe) ____ _
DATE: gj ~\{t3
pH BUFFER 7.0 -~7u ....... ooL_ __ _
BY:~..,y'----­
(Sampler's initials)
pH BUFFER 4.0 _4__._._.. 0..,__ __ _
SPECIFIC CONDUCTIVITY ----'tl.._9.._9...__ _____ ----*,uMH~~O~s
STEAM DEPTH: ~6~ t -.\
pHofWATER ___ :J~-~4=~-------
CONDcurnh==o=s-~~~~~0~­
pH Units __ _.._] ....... _L.\L-'1-'-----
coND~=mh=o=s--z~g~o~--
pH units __ ']........_.~ __.Lfuob"----
Comments:
'·
TEMP_~J~~~·-o~~=----
• I
COND~mh==o=s~~2~7~&~-
pH units ___ 7..&...:...-_\..j.:....7_,___
Temp oc ---=:J..=l.<..:::.'--'-0""-"'-K-
COND~=mh=o=s'----~~=g~~~-­
pH units __ _.7_..._'-1.._.6""-----
Temp °C ___ ,,...2_._1....._. -..._\ \.__
g-!21/1:3 Arc¥we.A oc-s\1-.c.. (!.<..+ OGH5. &....,.,..;"' .,__A Tr...,._ ... ,;.c pr-c....s.?A-t t:re.,;,IS w.v r:Ar-y {s.e..c. pv..:t~.
alz.~>lr3~ Arcivc;..o\ t).A si+e.r t23..-l-<'950 t:.rc;.s,.\<-WM J.:.r-y. S'?c f>l...o±o.
ql!oii3-Arr:ve.tA o"" s,'te__ o.-+ 1230 .. s~ples 1.....>er-e... c.c\\c.,L-±e.ol ..._t-
. !2..3£. Le..f ·l-s~te.. o-+ 12'-\0.
White Mesa Mill -Standard Operating Procedures
Book #11: Environmental Protection Manual, Section 2.1
Date: 2/07 Revision: DUSA-1
PageS of5
Attachment A
FIELD WATER ANALYSIS SURFACE WATER
WHITE MESA MILL
LOCATION (Circle one~nwood ~ Westwater Canyon Other (describe). ____ _
DATE:_-'-'H._../&c..?.._,·· ,r<-1 z ..... "'-'-'3-'-'-------
pH BUFFER 7.0 ___ 1-....:..=·0 __ _
BY: G.P.
(Sampler's initials)
pH BUFFER 4.0 __ _..:.y_, _o __ _
SPECIFIC CONDUCTIVITY ___ 't.:...Jtj'---'Cf ____ __!::uMH~~O~s
STEAM DEPTH:
pHofWATER __ ~7~-2q=5 __________ __ TEMP_~6~~=6~7 ____ __
• I
COND J.lmhos 4¢3.~ COND ~mhos 'io3;g:
pH Units __ J-""""'""--·q_FJ __ _ pH units ___ 1;..__._•1._..1 ____ _
Temp °C_--'~'*"-=G'""""'[ __ _
COND W!!bos L:io5.1 COND ~mhos 4ol.(.b
pH units _ ___,_7-.-=-· 'l"-"{S'------pH units __ __;--=1-.:....:.'....:.'i_..'i __ _
Temp °C ----'6=·="...L.r ____ __
Comments:
W€ \t._,.... Ceo .... ch1'"' 2 a..-<.. de •. ..-.::....-..d_ ~:-a'iit-"':5 • -t"r..,.., .. « U-€H...\"7 .~ (.,;..,..,""'-Q. ""-C
a.~c!.J>a.u\J.Twfr_ G'"">< pcrx:·~-\. l nl.li=<J """ Hk aA· t22i> r-J \..-.(:}
ATTACHMENT I
SOIL SAMPLE GRAPHS, DATA TABLE, LABORATORY RESULTS AND QAJQC
+ Ill I -;:: ......
+ Ill I < "'
+ Ill I < w
+ Ill I
1
+ Ill I -;::
(11
+ Ill I < m
0
!='
(11 ...... ......
<.n !\)
1\) (11 VJ
VJ <.n
Jul-98 -1------111r:,----.k----l-..---+----+--------~
Oct-98 -
Jan-99
Apr-99
Jul-99
Oct-99
Jan-00
Apr-00
Jul-00
Oct-00
Jan-01
Apr-01 -
Jul-01 -
Oct-01 -
Jan-02
Apr-02
Jul-02
Oct-02
Jan-03
Apr-03
Jul-03
Oct-03
Jan-04
Apr-04 -
Jul-04
Oct-04
Jan-05
Apr-05
Jul-05
Oct-05
Jan-06
Apr-06
Jul-06
Oct-06 -
Jan-07 -
Apr-07
Jul-07
Oct-07
Jan-08 -~
Apr-08 -
Jul-08
Oct-08 -;
Jan-09 -
Apr-09
Jul-09
Oct-09 -
Jan-1 0
Apr-10
Jul-10
Oct-10
Jan-11
Apr-11
Jul-11
Oct-11
Jan-12
Apr-12
Jul-12
Oct-12
Jan-13
Apr-13
Jul-13 I • 8... I e I I I I I
JJ m Q.
c
3 ~ 1\) en
0 0
::::J n C1)
::::J -""' m !:!:. 0
::::J tn
::::J en 0 -"C
0 :; -
p ...... [\) UJ 7'-
0 01 ...... 0, 1\) 01 UJ 0, .j::. 01
Jul-98
Oct-98
Jan-99
Apr-99 -
Jul-99
Oct-99 -
Jan-00 -
Apr-00 -
Jul-00
Oct-00
Jan-01
Apr-01
Jul-01
Oct-01
Jan-02
Apr-02
Jul-02
Oct-02 c:
+ Jan-03 ~ m
Apr-03 -::::s
OJ Jul-03 -I:
I Oct-o3 -3 -;:: Jan-04 I ...... z
Apr-04 -m
+ -Jul-04 -.
Oct-04 0
OJ Jan-05 0
I ::::s
< Apr-05 (')
' CD 1\) Jul-05 ::::s
Oct-05 -
+
~
Jan-06 -m ::::!'. Apr-06 -0 OJ Jul-06 ::::s I rn < Oct-06 -' w Jan-07 -::::s
+
Apr-07 -(/)
Jul-07 2.
OJ Oct-07 -I Jan-08 -"C
< Apr-08 • 0
.J:.. ;; Jul-08 -
+
Oct-08
Jan-09
OJ Apr-09 ·1 I < Jul-09 ~
' Oct-09 01
Jan-10 .,
+ Apr-1 0
Jul-10
OJ Oct-10 I Jan-11 < ' Apr-11 (J)
Jul-11
Oct-11
Jan-12
Apr-12
Jul-12
Oct-12
Jan-13
Apr-13
Jul-13
BHV-1
Date Ra-I U-Nat 226 I
917/80 0.650 0.420
9/8/81 0.400 1.800
12/3/81 0.790 0.770
6/30/82 0.423 0.384
5/5/83 0.471 0.410
6/4/84 0.713 0.866
10/12/84 2.960 0.886
8/28/85 1.630 0.800
8/1/86 0.369 0.654
8/17/87 0.600 0.800
8/28/88 1.500 1.600
8/25/88 1.200 1.600
8/1/90 2.900 5.800
8/5/91 3.900 8.800
8/13/92 1.200 2.200
8/13/93 2.000 1.700
8/3/94 1.000 1.600
8/28/95 2.810 4.700
8/13/96 1.700 2.150
8/1197 0.540 0.310
711/98 1.600 3.050
8/24/99 2.270 1.740
12/1100 1.510 1.210
8/23/01 1.000 1.000
8/1102 1.300 1.350
8/5/03 0.800 0.990
8/9/04 0.600 0.610
8/3/05 0.900 0.960
8/7/06 0.700 0.760
8/8/07 1.100 2.370
8/20/08 0.900 1.230
8/10/09 0.800 0.880
8/2/10 1.3 1.090
8/23/11 0.9 1.320
8/20/12 0.5 1.960
8/21/13 0.7 1.013
*Data not avm1able.
WHITE MESA MILL
Soil Sampling Results
(pCi/g)
BHY-2 BHV-3 BHV-4
Ra-U-Nat Ra-U-Nat Ra-U-Nat 226 226 226
0.340 0.420 0.420 0.420 0.410 12.194
0.300 0.600 0.300 0.600 0.200 3.000
0.440 0.560 0.890 0.420 0.750 0.630
0.412 0.180 0.265 0.207 0.478 0.260
0.569 0.550 0.461 0.340 0.643 0.340
0.618 0.683 0.489 0.471 0.124 0.324
2.330 0.069 2.880 0.721 3.490 0.804
2.190 0.424 2.270 0.424 4.330 0.294
0.466 0.866 0.382 0.694 0.396 0.826
1.500 0.900 0.800 0.600 1.200 0.700
1.300 0.700 0.600 0.900 1.000 1.300
1.100 3.000 0.800 1.000 1.100 1.400
1.000 1.400 0.800 1.400 1.800 1.300
1.700 2.600 2.600 5.700 1.800 2.600
0.900 1.400 0.800 1.200 0.900 0.900
1.400 1.700 1.100 1.900 0.800 1.600
0.700 0.800 0.700 0.900 0.700 1.100
0.680 0.200 0.880 0.650 0.580 0.240
0.600 0.460 0.300 0.210 0.500 0.520
0.560 0.160 0.410 0.270 0.410 0.260
0.700 0.580 0.500 0.450 1.000 1.190
0.780 0.840 0.530 0.420 0.840 0.770
0.810 0.530 * * 0.830 1.220
0.600 0.300 0.400 0.300 0.900 1.000
0.900 0.524 0.500 0.297 1.200 1.490
0.600 0.790 0.500 0.330 0.600 0.4300
0.400 0.250 0.400 0.220 0.600 0.5100
0.700 0.340 0.600 0.270 0.600 0.3800
0.440 0.250 0.410 0.250 0.520 0.480
0.700 0.530 0.200 0.550 0.500 0.740
0.300 0.430 0.600 0.980 0.500 0.790
0.700 0.540 0.700 1.080 0.800 0.610
1.0 1.490 0.8 0.62 1.3 1.69
0.4 0.320 0.4 0.4 0.5 0.58
0.4 0.540 0.7 1.09 0.6 0.81
0.3 0.405 0.6 1.35 0.3 0.54
BHV-5 BHY-6
Ra-U-Nat 1 Ra-U-Nat
226 ~ 226
0.230 14.89 - -
0.300 0.600 . -
0.550 0.420 --
0.449 0.216 -
0.147 0.140 ~ -
0.132 0.310 .
2.550 0.817 . -
1.280 0.577 --
0.728 0.836 --
1.500 1.300 . -
3.800 5.000 --
2.900 5.700 --
3.700 3.200 -
2.500 4.400 --
1.100 1.800 .
4.800 3.500 . -
3.000 3.800 . .
2.800 1.600 -.
1.900 2.010 . .
1.700 1.500 . -
3.000 2.760 --
3.270 3.150 . -
2.810 3.250 . -
1.200 1.100 --
2.400 2.810 60.00 0.550
0.280 0.420 0.600 0.530
1.000 1.400 0.900 1.400
0.700 0.410 1.000 1.200
1.400 1.300 0.780 0.650
1.100 1.450 0.800 0.930
0.800 1.330 0.500 0.670
2.600 2.980 0.500 0.810
1.7 1.69 0.8 0.87
1.0 1.48 0.6 0.86
1.6 2.70 0.8 1.37
1.1 1.62 0.5 0.743
HF.it:F.r.iffiflii!!!lia~ www.ener&Yieb.com
.,.,~,., 1111 Helella, llfri77-47Z-G711 • BJIIInp.IITIGI·UI-4418 • Catper, WY III-23HI11
Glllltll, WY 111-118-7171 • Rapid Cit)', SD 111-172·1221 • Collep StatiM, TX Hl-tiD-2218
September 13, 2013
Energy Fuels Resources (USA) Inc
6425 S Hwy 191
Blanding, UT 84511
Workorder No.: C13081040
Project Name: Annual Soil 2013
ANALYTICAL SUMMARY REPORT
Energy Laboratories, Inc. Casper WY received the following 8 samples for Energy Fuels Resources (USA) Inc on 8/27/2013
for analysis.
Sample ID Client Sample ID Collect Date Receive Date Matrix Test
C13081 040-001 BHV-1 08/21/13 9:40 08/27/13 Soil Uranium, Total
Digestion, Total Metals
Digestion For RadioChemistry
Radium 226
c 13081 040-002 BHV-2 08/21/13 9:50 08/27/13 Soil Same As Above
c 13081 040-003 BHV-3/Biack Mesa 08/21/13 10:30 08/27/13 Soil Same As Above
c 1 3081 040-004 BHV-4 08/21/13 9:30 08/27/13 Soil Same As Above
c 13081 040-005 BHV-5 08/21/13 9:10 08/27/13 Soil Same As Above
c 13081 040-006 BHV-6 08/21/13 9:00 08/27/13 Soil Same As Above
C13081 040-007 Westwater 08/21/13 10:45 08/27/13 Soil Same As Above
c 13081 040-008 BHV-65 08/21/13 10:30 08/27/13 Soil Same As Above
The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were
performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted.
Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601,
unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical
Report, the QNQC Summary Report, or the Case Narrative.
If you have any questions regarding these test results, please call.
Report Approved By: Digitally signed by
Sheri M. Mead
Date: 2013.09.1316:40:13-06:00
Page 1 of 14
Heleaa, MT817-472-G711 • Blllinp, MT 8GI-731-44H • Catpar, WY 811-231-1515
Glllltle, WY 81&-IM-7175 • fla hi C ,SD 118-172-1225 • eolleaeSI4tion, TX 88HID-2%18
CLIENT: Energy Fuels Resources (USA) Inc
Project: Annual Soil 2013 Report Date: 09/13/13
Sample Delivery Group: C13081 040 CASE NARRATIVE
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are
hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has
begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for
seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria
for PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize
its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r-Energy Laboratories, Inc. -Rapid City, SD
eli-cs-Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
US EPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA;
Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify Ell's certification coverage by visiting www.energylab.com
Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 14
EN:RGY
' ''I
Helella, MT 871-472-8711 • Blllinp, MT IGI-731-4481 • Cuper, WY 881-235-ISU
Glllettl, WYIU-III-7171 • Rapid City, SD 888-172·1221 • Coll.,eStation, TX 881-110.2218
LABORATORY ANAL VTICAL REPORT
Client:
Prepared by Casper, WY Branch
Energy Fuels Resources (USA) Inc Report Date: 09/13/13
Collection Date: 08/21/13 09:40
DateReceived: 08/27/13
Matrix: Soil
Project:
lab ID:
Client Sample ID
Analyses
METALS· TOTAL
Uranium
RADIONUCLIDES
Radium 226
Annual Soil 2013
C13081 040-001
BHV-1
Radium 226 precision (±)
Radium 226 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
1.5 mglkg-dry
0.7 pCilg-dry
0.06 pCi/g-dry
0.02 pCi/g-dry
MDC -Minimum detectable concentration
Qualifiers
D
MCL/
RL QCL Method
0.1 SW6020
E903.0
E903.0
E903.0
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Analysis Date I By
08/31/13 01:02 / cp
09111113 22:04 / Irs
09/11 /13 22:04 I trs
09/11113 22:04 I Irs
Page 3 of 14
EN:RGY
~-'-! ' I
Helw, liT 877-472-8711 • Bllllnp, liT IIGI-735-4481 • Cuper, WY 811-235-0515
Gillette, WYIU-188·7175 • Rapid CltJ, SD 111-172-1225 • Colleae Station, TX 111-IID-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 09/13/13
Collection Date: 08/21/13 09:50
DateRece ived: 08/27 I 13
Matrix: Soil
Project: Annual Soil 201 3
Lab ID: c 13081 040-002
Client Sample ID BHV-2
Analyses
METALS· TOTAL
Uranium
RADIONUCLIDES
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
0.6 mglkg-dry
0.3 pCilg-dry
0.04 pCilg-dry
0.03 pCilg-dry
MDC -Minimum detectable concentration
Qualifiers
D
MCU
RL QCL Method
0.1 SW6020
E903.0
E903.0
E903.0
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
0 -RL increased due to sample matrix.
Analysis Date I By
08131113 01 :11 1cp
09111113 22:04 I trs
09111113 22:04 I trs
09111113 22:04 I trs
Page 4 of 14
EI\ERGY
-. • ' I
Helella, IT 871-472-8711 • Bllllnp, IT 808-7al-4481 • Caspar, WY 811-235-1111
Gillette, W'f IH-118· 7171 • Rapid City, SD 188-172·1221 • Collap Station, TX 881-tiD-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 09/13/13
Collection Date: 08/21/13 10:30
DateReceived: 08/27/13
Matrix: Soil
Project: Annual Soil 2013
Lab ID: C13081 040-003
Client Sample ID BHV-3/Biack Mesa
Analyses
METALS· TOTAL
Uranium
RADIONUCLIDES
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL -Quality control limit.
Result Units
2.0 mglkg-dry
0.6 pCilg-dry
0.06 pCilg-dry
0.03 pCilg-dry
MDC -Minimum detectable concentration
Qualifiers
0
MCU
RL QCL Method
0.1 SW6020
E903.0
E903.0
E903.0
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Analysis Date I By
08131113 01 :15 I cp
09111 113 22:04 I trs
09111113 22:04 I Irs
09111113 22:04 I trs
Page 5 of 14
EN:RGY
~ -. , l r •I
Helen•, MT 817-472-0111 • Bllllnp, MT 801·731-4411 • Casper, WY 111-231-0511
Gillllh, WY 111-111·7171 • Rapld City, SD 111-172·1225 • Collqe Station, TX 811-tiiJ-2211
LABORATORY ANALYTICAL REPORT
Client:
Prepared by Casper, WY Branch
Energy Fuels Resources (USA) Inc Report Date: 09/13/13
Collection Date: 08/21/13 09:30
DateReceived: 08/27/13
Matrix: Soil
Project: Annual Soil 2013
Lab ID: c 13081 040-004
Client Sample ID BHV-4
Analyses
METALS· TOTAL
Uranium
RADIONUCLIDES
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
0.8 mglkg-dry
0.3 pCi/g-dry
0.05 pCi/g-dry
0.03 pCi/g-dry
MDC-Minimum detectable concentration
Qualifiers
D
MCL/
RL QCL Method
0.1 SW6020
E903.0
E903.0
E903.0
MCL-Maximum contaminant level.
NO -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Analysis Date I By
08/31/13 01:19 / cp
09/11/13 22:04/trs
09/11/13 22:04 /Irs
09/11/13 22:04/ trs
Page 6 of 14
EN:RGY
.' -•• 1 / • I•!
Helene, MT 877-472.0711 • Blllln&a, MT BGI-m-44at • Cupar, WY 881-235--8511
Gillette, WY 118-118·7171 • Rapid City, SD 818·172·1221 • Coll1188 Station, TX 811-tiD-2218
LABORATORY ANALYTICAL REPORT
Client:
Prepared by Casper, WY Branch
Energy Fuels Resources (USA) Inc Report Date: 09/13/13
Collection Date: 08/21/13 09:1 o
DateRece ived: 08/27 I 1 3
Matrix: Soil
Project: Annual Soil 2013
LabiD: c 13081 040-005
Client Sample ID BHV-5
Analyses
METALS· TOTAL
Uranium
RADIONUCLIDES
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
2.4 mglkg-dry
1.1 pCi/g-dry
0.09 pCi/g-dry
0.03 pCi/g-dry
MDC -Minimum detectable concentration
Qualifiers
D
MCL/
RL QCL Method Analysis Date I By
0.1 SW6020 08/31/13 01 :54/ cp
E903.0 09/11/13 23:40 I trs
E903.0 09/11/13 23:40 I trs
E903.0 09/11/13 23:40 I trs
MCL-Maximum contaminant level.
NO -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Page 7 of 14
EI\ERGY
/ -: . ' ~ '.'
Helena, MT 877-472-0711 • Billings, MT 801·735-4481 • Cupar, WY 881-23H515
Gillette, WY 816-188·7175 • Rapid City, SD 188·872·1225 • Collep Station, TX III-IID-2218
LABORATORY ANALYTICAL REPORT
Client:
Prepared by Casper, WY Branch
Energy Fuels Resources (USA) Inc Report Date: 09/13/13
Collection Date: 08/21/13 09:00
DateReceived: 08/27/13
Matrix: Soil
Project: Annual Soil 2013
LabiD: C13081 040-006
Client Sample ID BHV-6
Analyses
METALS· TOTAL
Uranium
RADIONUCLIDES
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
1.1 mglkg-dry
0.5 pCilg-dry
0.05 pCilg-dry
0.02 pCilg-dry
MDC -Minimum detectable concentration
Qualifiers
D
MCLI
RL QCL Method
0.1 SW6020
E903.0
E903.0
E903.0
MCL -Maximum contaminant level.
NO-Not detected at the reporting limit.
D -RL increased due to sample matrix.
Analysis Date I By
08131113 01:241 cp
09111113 23:40 I trs
09111113 23:40 I trs
09111113 23:40 I trs
Page 8 of 14
Helena, MT 877-472.0711 • Bllllnp, MT IGI-731-4411 • Cuper, WY 111-235-1515
Gllltttt, WY 816-188-7175 • Rapid City, SD 186-872·1225 • Colleae Station, 1X 811-&10-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 09/13/13
Collection Date: 08/21/13 10:45
DateReceived: 08/27/13
Matrix: Soil
Project:
lab ID:
Annual Soil 2013
c 13081 040-007
Client Sample ID Westwater
Analyses
METALS· TOTAL
Uranium
RADIONUCLIDES
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality contrOl limit.
Result Units
ND mg/kg-dry
0.07 pCilg-dry
0.02 pCilg-dry
0.02 pCilg-dry
MDC -Minimum detectable concentration
Qualifiers
D
MCU
RL QCL Method
0.1 SW6020
E903.0
E903.0
E903.0
MCL-Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Analysis Date I By
08/31113 01:46 1 cp
09111113 23:40 I trs
09111113 23:40 I trs
09111113 23:40 I trs
Page 9 of 14
Helena, MT 877-472-0711 • Bllllnas, MT 801·731-4481 • Casper, WY 811-231-1515
Gllltltl, WV 818-188·7171 • Rapid City, SD 888-172·1225 • Collace Stati011, TX 881-810-2218
LABORATORY ANALYTICAL REPORT
Client:
Prepared by Casper, WY Branch
Energy Fuels Resources (USA) Inc Report Date: 09/13/13
Collection Date: 08/21/13 10:30
DateReceived: 08/27/13
Matrix: Soil
Project: Annual Soil 2013
Lab ID: c 13081 040-008
Client Sample ID BHV-65
Analyses
METALS-TOTAL
Uranium
RADIONUCLIDES
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
1.3 mglkg-dry
0.7 pCilg-dry
0.06 pCilg-dry
0.02 pCilg-dry
MDC-Minimum detectable concentration
Qualifiers
D
MCU
RL QCL Method
0.1 SW6020
E903.0
E903.0
E903.0
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
D -RL increased due to sample matrix.
Analysis Date I By
08131113 01:50 I cp
09111113 23:40 I trs
09111113 23:40 I trs
09111113 23:40 I trs
Page10of14
EN:RGY
·-; ,,j
Helena, Ill' 877-472-0711 • Bllllnaa, Ill' 8GI·735-4.tltl • Casper, WY 811-235-1515
Gillette, WV 111-188· 7171 • Rapid City, SD 181-172·1221 • College Station, 1X 111-110-2211
QAJQC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Soil 2013
Report Date: 09/13/13
Work Order: C13081 040
Analyte Count Result Units
Method: E903.0
Sample 10: C13081039·002AMS
Radium 226
Sample 10: C13081039-002AMSO
Radium 226
Sample 10: LCS-38833
Radium 226
Sample 10: MB-38833
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Qualifiers:
RL-Analyte reporting limit.
3
MDC-Minimum detectable concentration
Sample Matrix Spike
4.8 pCi/g-dry
Sample Matrix Spike Duplicate
4.4 pCi/g-dry
Laboratory Control Sample
0.6 pCi/g-dry
Method Blank
0.0 pCilg-dry
0.0 pCi/g-dry
0.0 pCi/g-dry
RL %REC Low Limit High Limit RPO RPOLimlt Qual
Run: BERTHOLD 770-2_130830B
128 70 130
Run : BERTHOLD 770-2_130830B
116 70 130 8.4
Run: BERTHOLD 770-2_130830B
118 80 120
Run: BERTHOLD 770-2_130830B
NO-Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Batch: 38833
09/11/13 22:04
09/11/13 22:04
19.7
09/11 /13 23:40
09/11 /13 23:40
u
Page 11 of 14
EI\ERGY
·-;., ;r. '
Helena, MT 817-472-11711 • BllllnJI, MT IGI-731-4481 • Casper, WY 111-235-1111
Gillette, WY 111-118·7171 • Rapid City, SD 111-172-1221 • Colleae Station, IX 811-110-2211
QAJQC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: Annual Soil 2013
Report Date: 09/13/13
Work Order: C13081040
Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimlt Qual
Method: SW6020 Analytical Run: ICPMS4-C_130830A
Sample ID: ICV Initial Calibration Verification Standard 08/30/13 14:19
Uranium 0.0491 mg/L 0.00030 98 90 110
Sample ID: ICSA Interference Check Sample A 08/30/13 14:23
Uranium 5.08E-05 mg/L 0.00030
Sample ID: ICSAB Interference Check Sample AB 08/30/13 14:27
Uranium 1.15E-05 mg/L 0.00030
Method: SW6020 Batch: 38856
Sample ID: MB-38856 Method Blank Run: ICPMS4-C_130830A 08/31/13 00:02
Uranium NO mg/kg-dry 0.10
Sample ID: LFB-38856 Laboratory Fortified Blank Run: ICPMS4-C_130830A 08/31/13 00:06
Uranium 25.9 mg/kg-dry 0.15 104 75 125
Sample ID: LCS3-38856 Laboratory Control Sample Run: ICPMS4-C_130830A 08/31/13 00:10
Uranium 116 mg/kg-dry 0.37 113 75 125
Sample ID: C13081 040-001 A OIL Serial Dilution Run: ICPMS4-C_130830A 08/31/13 01:06
Uranium 1.40 mg/kg-dry 0.75 7.1 10
Sample ID: C13081 040-005AMS3 Sample Matrix Spike Run: ICPMS4-C_130830A 08/31/13 01 :59
Uranium 29.3 mg/kg-dry 0.15 108 75 125
Sample ID: C13081 040-005AMSD3 Sample Matrix Spike Duplicate Run: ICPMS4-C_130830A 08/31/13 02:03
Uranium 28.7 mg/kg-dry 0.15 105 75 125 2.0 20
Qualifiers:
RL-Analyte reporting limit. NO -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 12 of 14
EI\ERGY Helena, 11fT 877-472-0711 • Billings, 11fT BGD-735-4489 • Cuper, WY 818-231-1115
Gillette, W'f 118-188-7175 • Rapid City, SD 818·172-1225 • College Station, 1X 818-6111-2211
Standard Reporting Procedures
Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual
Chlorine, are qualified as being analyzed outside of recommended holding time.
Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry.
For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis.
Workorder Receipt Checklist
Energy Fuels Resources (USA) Inc
Login completed by; Tessa Parke
Reviewed by: BL2000\kmiller
Reviewed Date: 8/28/2013
Shipping container/cooler in good condition?
Custody seals intact on all shipping container(s)/cooler(s)?
Custody seals intact on all sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
(Exclude analyses that are considered field parameters
such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.)
Temp Blank received in all shipping container(s)/cooler(s)?
Container/Temp Blank temperature:
Water-VOA vials have zero headspace?
Water-pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0
Yes 0
Yes D
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
25.8"C
Yes D
Yes 0
C13081040
Date Received: 8/27/2013
Received by: cav
No 0
NoD
NoD
NoD
No 0
NoD
NoD
NoD
NoD
NoD
NoD
NoD
No 0
Carrier Next Day Air
name:
Not Present D
Not Present D
Not Present 0
Not Applicable 0
NoVOA vials submitted 0
Not Applicable 0
Page 13 of 14
Sheet 1 of 1
CHAIN OF CUSTODY
Samples Shipped to: Energy Laboratories Contact: Garrin Palmer -=2:..:..;39.=;3;_jjS~o.;;;;.u.;;;;th~C;;;,;re;,;..e~k;;.,;;H,.,..W'""Y,.,.-----Ph: 435 678 2108
Casper, WY 82601 [e-mail]
Chain of Custody/Sampling Analysis Request
p . t rojec
Annual Soils 2013
Da1e
SBmpleiD Collected
BHV-1 8/21/2013
BHV-2 8/21/2013
BHV -3/Biack Mesa 8/21./2013
BHV-4 8/21/2013
BHV-5 8/21/2013
BHV-6 8/21/2013
Westwater 8/21/2013
BHV-65 8/21/2013
Comments:
Relinquished By:(Signature}
s amp1ers N a me s amp1ers s· t 1gna ure
Garrin Palmer ~ ,A A .A,..(_ fivv--
Time
Collected Laboratory Analysis Requested
940 Ra-226, U-Nat
950 Ra-226, U·Nat
1030 Ra-226, U-Nat
930 Ra-226, U-Nat
910 Ra-226, U-Nat
900 Ra-226, U-Nat
1045 Ra-226, U·Nat
1030 Ra-226 U-Nat
Date/Time Received By:{Signatur-e) Datemme
8/2212013
1200
Datemme
Ct3o8ftX/D
Page 14 of 14