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HomeMy WebLinkAboutDRC-2014-001902 - 0901a0688040a01eENERGYFUELS Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www energvfuels.com Mr. Rusty Lundberg Division of Radiation Control Utah Department of Environmental Quality 195 North 1950 West February 21, 2014 DRC"201 4-001 902 Sent VIA OVERNIGHT DELIVERY P.O. Box 144850 Salt Lake City, UT 84114-4820 Re: Transmittal of 4th Quarter 2013 Nitrate Monitoring Report Stipulation and Consent Order Docket Number UGW12-04 White Mesa Uranium Mill Dear Mr. Lundberg: Enclosed are two copies of the White Mesa Uranium Mill Nitrate Monitoring Report for the 4th Quarter of 2013 as required by the Stipulation and Consent Order Docket Number UGW12-04, as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours very truly, ENERGY FUELS RESOURCES (USA) INC. Kathy Weinel Quality Assurance Manager cc: David C. Frydenlund Dan Hillsten Harold R. Roberts David E. Turk Frank Filas White Mesa Uranium Mill Nitrate Monitoring Report State of Utah Stipulated Consent Agreement, January 2009 Docket No. UGW09-03 4th Quarter (October through December) 2013 Prepared by: Energy Fuels Resources (USA) Inc. 225 Union Boulevard, Suite 600 Lakewood, CO 80228 February 21, 2014 TABLE OF CONTENTS 1.0 INTRODUCTION ................................................................................................. 1 2.0 GROUNDWATER NITRATE MONITORING ................................................ ! 2.1 Samples and Measurements Taken During the Quarter ..................................... 1 2.1.1 Nitrate Monitoring ..................................................................................... 2 2.1.2 Parameters Analyzed .................................................................................. 3 2.1.3 Groundwater Head and Level Monitoring ................................................. -. 3 2.2 Sampling Methodology and Equipment and Decontamination Procedures ....... 3 2.2.1 Well Purging, Sampling and Depth to Groundwater .................................. 4 2.2.2 Piezometer Sampling .................................................................................. 5 2.3 Field Data ............................................................................................................ 5 2.4 Depth to Groundwater Data and Water Table Contour Map .............................. 5 2.5 Laboratory Results .............................................................................................. 5 2.5.1 Copy of Laboratory Results ........................................................................ 5 2.5.2 Regulatory Framework ............................................................................... 5 3.0 QUALITY ASSURANCE AND DATA VALIDATION ................................... 6 3.1 Field QC Samples ................................................................................................ 6 3.2 Adherence to Mill Sampling SOPs ..................................................................... 6 3.3 Analyte Completeness Review ................... ,. ....................................................... 7 3.4 Data Validation .................................................................................................... 7 3.4.1 Field Data QA/QC Evaluation .................................................................... 7 3.4.2 Holding Time Evaluation ............................................................................ 8 3.4.3 Analytical Method Checklist ...................................................................... 8 3.4.4 Reporting Limit Evaluation ........................................................................ 8 3.4.5 QA/QC Evaluation for Sample Duplicates ................................................. 9 3.4.6 Other Laboratory QA/QC ........................................................................... , 9 3.4.7 Receipt Temperature Evaluation ............................................................... 10 3.4.8 Rinsate Check ........................................................................................... 10 4.0 INTERPRETATION OF DATA ....................................................................... 10 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions ........... 10 4.1.1 Current Site Groundwater Contour Map ................................................... 10 4.1.2 Comparison of Current Groundwater Contour Map to Groundwater Contour Map for Previous Quarter.................................................................................. 13 4.1.3 Hydrographs .............................................................................................. 15 4.1.4 Depth to Groundwater Measured and Groundwater Elevation ................. 15 4.2 Effectiveness of Hydraulic Containment and Capture ...................................... 15 4.2.1 Hydraulic Containment and Control ......................................................... 15 4.2.2 Current Nitrate and Chloride Isoconcentration Maps ............................... 18 4.2.3 Comparison of Areal Extent ............................................................................ 18 4.2.4 Nitrate and Chloride Concentration Trend Data and Graphs .................... 19 4.2.5 Interpretation of Analytical Data .............................................................. 19 4.3 Estimation of Pumped Nitrate Mass and Residual Nitrate Mass within the Plume .......................................................................................................................... 21 5.0 LONG TERM PUMP TEST AT TWN-02, TW4-22, TW4-24, and TW4-25 OPERATIONS REPORT .................................................................................. 23 5.1 Introduction ....................................................................................................... 23 1 5.2 Pumping Well Data Collection ......................................................................... 23 5.3 Water Level Measurements .............................................................................. 23 5.4 Pumping Rates and Volumes ................................... , ......................................... 24 6.0 CORRECTIVE ACTION REPORT ................................................................. 24 6.1 Assessment of Previous Quarter's Corrective Actions ..................................... 24 7.0 CONCLUSIONS AND RECOMMENDATIONS ............................................ 24 8.0 ELECTRONIC DATA FILES AND FORMAT .............................................. 29 9.0 SIGNATURE AND CERTIFICATION ........................................................... 30 Table 1 Table 2 Table 3 Table 4 Table 5 Table 6 Table 7 Table 8 LIST OF TABLES Summary of Well Sampling and Constituents for the Period Nitrate Mass Removal Per Well Per Quarter Nitrate Well Pumping Rates and Volumes Quarterly Calculation of Nitrate mass Removed and Total Volume of Water Pumped Nitrate Data Over Time for MW-30, MW-31, MW-5, and MW-11 Slug Test Results Pre-Pumping Saturated Thickness Pre-Pumping Hydraulic Gradients and Flow Calculations ii INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and Field Data Worksheets Tab C Kriged Current Quarter Groundwater Contour Map and Weekly, Monthly and Quarterly Depth to Water Data Tab D Kriged Previous Quarter Groundwater Contour Map Tab E Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells Tab F Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Tab G Laboratory Analytical Reports Tab H Quality Assurance and Data Validation Tables H-1 Field Data QA/QC Evaluation H-2 Holding Time Evaluation H-3 Analytical Method Check H-4 Reporting Limit Evaluation H-5 QAJQC Evaluation for Sample Duplicates H-6 QC Control limits for Analysis and Blanks H-7 Receipt Temperature Evaluation H-8 Rinsate Evaluation Tab I Kriged Current Quarter Nitrate and Chloride Isoconcentration Maps Tab J Analyte Concentration Data Over Time Tab K Nitrate and Chloride Concentration Trend Graphs Tab L CSV Transmittal Letter iii AWAL CA CAP CIR DIFB DRC EFRI ft amsl GWDP LCS MS MSD QA QAP QC RPD sco SOPs UDEQ voc ACRONYM LIST American West Analytical Laboratory Consent Agreement Corrective Action Plan Contamination Investigation Report Deionized Field Blanks Utah Division of Radiation Control Energy Fuels Resources (USA) Inc. feet above mean sea level Groundwater Discharge Permit Laboratory Control Spike Matrix Spike Matrix Spike Duplicate Quality Assurance Groundwater Monitoring Quality Assurance Plan Quality Control Relative Percent Difference Stipulated Consent Order Standard Operating Procedures Utah Department of Environmental Quality Volatile Organic Compounds IV 1.0 INTRODUCTION The Utah Department of Environmental Quality ("UDEQ") Division of Radiation Control ("DRC") noted in a Request dated September 30, 2008 (the "Request"), for a Voluntary Plan and Schedule to Investigate and Remediate Nitrate Contamination at the White Mesa Uranium Mill (the "Mill") (the "Plan"), that nitrate levels have exceeded the State water quality standard of 10 mg/L in certain monitoring wells. As a result of the Request, Energy Fuels Resources (USA) Inc. ("EFRI") entered into a Stipulated Consent Agreement with the Utah Water Quality Board in January 2009 which directed the preparation of a Nitrate Contamination Investigation Report ("CIR"). A subsequent letter dated December 1, 2009, among other things, recommended that EFRI also address elevated chloride concentrations in the CIR. The Stipulated Consent Agreement was amended in August 2011. Under the amended Consent Agreement ("CA"), EFRI submitted a Corrective Action Plan ("CAP"), pursuant to the requirements of the Utah Groundwater Quality Protection Rules [UAC R317-6-6.15(C-E)] on November 29, 2011 and revised versions of the CAP on February 27, 2012 and May 7, 2012. On December 12, 2012, DRC signed the Stipulation and Consent Order ("SCO"), Docket Number UGW12-04, which approved the EFRI CAP, dated May 7, 2012. The SCO ordered EFRI to fully implement all elements of the May 7, 2012 CAP. Based on the schedule included in the CAP and as delineated and approved by the SCO, all activities associated with the implementation of the CAP began in January 2013. The reporting requirements specified in the CAP and SCO are included in this quarterly nitrate report. This is the Quarterly Nitrate Monitoring Report, as required under the SCO, State of UDEQ Docket No. UGW12-04 for the fourth quarter of 2013. This report meets the requirements of the SCO, State of UDEQ Docket No. UGW12-04 and is the document which covers nitrate corrective action and monitoring activities during the fomth quarter of 2013. 2.0 GROUNDWATER NITRATE MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of all groundwater monitoring wells, piezometers, existing wells, temporary chloroform contaminant investigation wells and temporary nitrate investigation wells is attached under Tab A. Nitrate samples and measurements taken during this reporting period are discussed in the remainder of this section. 1 2.1.1 Nitrate Monitoring Quarterly sampling for nitrate monitoring parameters was performed in the following wells: TWN-1 TWN-2 TWN-3 TWN-4 TWN-7 TWN-18 TW4-22* TW4-24* TW4-25* Piezometer 1 Piezometer 2 Piezometer 3 As discussed in Section 2.1.2 the analytical constituents required by the CAP are inorganic chloride and nitrate+nitrite as N (referred to as nitrate in this document) * Wells TW4-22, TW4-24, TW4-25 are chloroform investigation wells (wells installed and sampled primarily for the chloroform investigation) and are sampled as part of the chloroform program. The analytical suite for these three wells includes nitrate, chloride and a select list of Volatile Organic Compounds ("VOCs") as specified in the chloroform program. These three wells are included here because they are being pumped as part of the remediation of the nitrate contamination as required by the SCO and the CAP. The nitrate and chloride data are included in this report as well as in the chloroform program quarterly report. The VOC data for these three wells will be reported in the chloroform quarterly monitoring report only. The December 12, 2012 SCO approved the CAP, which specified the cessation of sampling in TWN-5, TWN-6, TWN-8, TWN-9, TWN-10, TWN-11, TWN-12, TWN-13, TWN-14, TWN-15, TWN-16, TWN-17, and TWN-19. Per the CAP and SCO, these wells were not sampled during this quarter. Additionally, the CAP and SCO approved the abandonment of TWN-5, TWN-8, TWN-9, TWN-10, TWN-11, TWN-12, TWN-13, TWN-15, and TWN-17 within 1 year of the SCO approval. These wells were abandoned in accordance with the DRC-approved Well Abandonment Procedure on July 31, 2013. Wells TWN-6, TWN-14, TWN-16, and TWN-19 have been maintained for depth to groundwater monitoring only, as noted in the CAP. Table 1 provides an overview of all locations sampled during the current period, along with the date samples were collected from each location, and the date(s) upon which analytical data were received from the contract laboratory. Table 1 also identifies rinsate samples collected, as well as sample numbers associated with any required duplicates. As indicated in Table 1, nitrate monitoring was performed in the nitrate monitoring wells, chloroform wells TW4-22, TW4-24, TW4-25 and Piezometers 1, 2, and 3. Analytical data for all of the above-listed wells, and the piezometers, are included in Tab G. Nitrate and chloride are also monitored in all of the Mill's groundwater monitoring wells and chloroform investigation wells. Data from those wells for this quarter are incorporated in certain maps and figures in this report but are discussed in their respective programmatic reports. 2 2.1.2 Parameters Analyzed Locations sampled during this reporting period were analyzed for the following constituents: • Inorganic Chloride • Nitrate plus Nitrite as Nitrogen (referred to herein as nitrate) Use of analytical methods consistent with the requirements found in the White Mesa Mill Groundwater Quality Assurance Plan, ("QAP") Revision 7.2, dated June 6, 2012 was confirmed for all analytes, as discussed later in this report. 2.1.3 Groundwater Head and Level Monitoring Depth to groundwater was measured in the following wells and/or piezometers, pursuant to Part I.E.3 of the Groundwater Discharge Permit ("GWDP") (dated August 24, 2012): • The quarterly groundwater compliance monitoring wells • Existing well MW -4 and all of the temporary chloroform investigation wells • Piezometers-P-1, P-2, P-3, P-4 and P-5 • MW-20, MW-22, and MW-34 • The DR piezometers that were installed during the Southwest Hydrogeologic Investigation • Nitrate wells TWN-01 , TWN-02, TWN-03, TWN-04, TWN-06, TWN-07, TWN-14, TWN-16, TWN-18 and TWN-19 In addition to the above, depth to water measurements are routinely observed in conjunction with sampling events for all wells sampled during quarterly and accelerated efforts, regardless of the sampling purpose. All well levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab C. Field data sheets for groundwater measurements are also provided in Tab C. Weekly and monthly depth to groundwater measurements were taken in the chloroform pumping wells MW-4, MW-26, TW4-19, TW4-20, and TW4-4, and the nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2. In addition, monthly water level measurements were taken in non-pumping wells MW-27, MW-30, MW-31, TW4-21, TWN-1, TWN-3, TWN-4, TWN-7, and TWN-18 as required by the CAP. 2.2 Sampling Methodology and Equipment and Decontamination Procedures The QAP provides a detailed presentation of procedures utilized for groundwater sampling activities under the GWDP (August 24, 2012). The sampling methodology, equipment and decontamination procedures that were performed for the nitrate contaminant investigation, as summarized below, are consistent with the QAP. 3 2.2.1 Well Purging, Sampling and Depth to Groundwater A list of the wells in order of increasing nitrate contamination is generated quarterly. The order for purging is thus established. The list is included with the Field Data Worksheets under Tab B. Mill personnel start purging with all of the nondetect wells and then move to the wells with detectable nitrate concentrations, progressing from the wells having the lowest nitrate contamination to wells with the highest nitrate contamination. Before leaving the Mill office, the pump and hose are decontaminated using the cleaning agents described in Attachment 2-2 of the QAP. Rinsate blanks are collected at a frequency of one rinsate per 20 field samples. Purging is completed to remove stagnant water from the casing and to assure that representative samples of formation water are collected for analysis. There are three purging strategies specified in the QAP that are used to remove stagnant water from the casing during groundwater sampling at the Mill. The three strategies are as follows: 1. Purging three well casing volumes with a single measurement of field parameters 2. Purging two casing volumes with stable field parameters (within 10% Relative Percent Difference ["RPD"]) 3. Purging a well to dryness and stability (within 10% RPD) of a limited list of field parameters after recovery. Mill personnel proceed to the first well, which is the well with the lowest concentration (i.e. non- dectect) of nitrate based on the previous quarter's sampling results. Well depth measurements are taken and the one casing volume is calculated. The purging strategy that will be used for the well is determined at this time based on the depth to water measurement and the previous production of the well. The Grundfos pump (a 6 to 10 gallon per minute [gpm] pump) is then lowered to the appropriate depth in the well and purging is started. At the first well, the purge rate is measured for the purging event by using a calibrated 5 gallon bucket. After the evacuation of the well has been completed, the well is sampled when possible, and the pump is removed from the well and the process is repeated at each well location moving from the least contaminated to most contaminated well. If sample collection is not possible due to the well being purged dry, a sample is collected after recovery using a disposable bailer and as described in Attachment 2-3 of the QAP. Sample collection follows the procedures described in Attachment 2-4 of the QAP. After the samples have been collected for a particular well, the samples are placed into a cooler that contains ice. The well is then recapped and Mill personnel proceed to the next well. If a bailer has been used it is disposed of. Decontamination of non-dedicated equipment, using the reagents in Attachment 2-2 of the QAP, is performed between each sample location, and at the beginning of each sampling day, in addition to the pre-event decontamination described above. 4 2.2.2 Piezometer Sampling Samples are collected from Piezometers 1, 2 and 3, if possible. Samples are collected from piezometers using a disposable bailer after one set of field measurements have been collected. Due to the difficulty in obtaining samples from the piezometers, the purging protocols set out in the QAP are not followed. After samples are collected, the bailer is disposed of and samples are placed into a cooler containing ice for sample preservation and transit to the Mill's contract analytical laboratory, American West Analytical Laboratories ("AWAL"). 2.3 Field Data Attached under Tab B are copies of all Field Data Worksheets that were completed during the quarter for the nitrate investigation monitoring wells and piezometers identified in Section 2.1.1 and Table 1. 2.4 Depth to Groundwater Data and Water Table Contour Map Depth-to-groundwater measurements that were utilized for groundwater contours are included on the Quarterly Depth to Water Sheet at Tab C of this Report along with the kriged groundwater contour map for the current quarter generated from this data. All well levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab C. A copy of the kriged groundwater contour map generated from the previous quarter's data is provided under Tab D. 2.5 Laboratory Results 2.5.1 Copy of Laboratory Results The analytical results were provided by AW AL. Table 1 lists the dates when analytical results were reported to the Quality Assurance ("QA") Manager for each well or other sample. Analytical results for the samples collected for this quarter's nitrate investigation and a limited list of chloroform investigation nitrate and chloride results are provided under Tab G of this Report. Also included under Tab G are the results of analyses for duplicate samples and rinsate samples for this sampling effort, as identified in Table 1. See the Groundwater Monitoring Report and Chloroform Monitoring Report for this quarter for nitrate and chloroform analytical results for the groundwater monitoring wells and chloroform investigation wells not listed in Table 1. 2.5.2 Regulatory Framework As discussed in Section 1.0 above, the Request, Plan, and CA each triggered a series of actions on EFRI's part. Potential surficial sources of nitrate and chloride have been described in the December 30, 2009 CIR and additional investigations into potential sources were completed and discussed with DRC in 2011. Pursuant to theCA, the CAP was submitted to the Director of the Division of Radiation Control (the "Director") on May 7, 2012. The CAP describes activities 5 associated with the nitrate in groundwater. The CAP was approved by the Director on December 12, 2012. This quarterly report documents the monitoring consistent with the program described in the CAP. 3.0 QUALITY ASSURANCEANDDATA VALIDATION EFRI' s QA Manager performed a QA/Quality Control ("QC") review to confirm compliance of the monitoring program with the requirements of the QAP. As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and QC review of laboratory data methods and data. Identification of field QC samples collected and analyzed is provided in Section 3 .1. Discussion of adherence to Mill sampling Standard Operating Procedures ("SOPs") is provided in Section 3.2. Analytical completeness review results are provided in Section 3.3. The steps and tests applied to check field data QA/QC, holding times, receipt temperature and laboratory data QA/QC are discussed in Sections 3.4.1 through 3.4.7 below. The analytical laboratory has provided summary reports of the analytical QA/QC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference certification and reporting protocol. The Analytical Laboratory QA/QC Summary Reports, including copies of the Mill's Chain of Custody and Analytical Request Record forms for each set of Analytical Results, follow the analytical results under Tab G. Results of the review of the laboratory QA/QC information are provided under Tab H and discussed in Section 3.4, below. 3.1 Field QC Samples The following QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program. Field QC samples for the nitrate investigation program consist of one field duplicate sample for each 20 samples, DI Field Blanks ("DIFB"), and equipment rinsate samples. During the quarter, one duplicate sample was collected as indicated in Table 1. The duplicate was sent blind to the analytical laboratory and analyzed for the same parameters as the nitrate wells. One rinsate blank sample was collected as indicated on Table 1. Rinsate samples are labeled with the name of the subsequently purged well with a terminal letter "R" added (e.g. TWN-7R). The field QC sample results are included with the routine analyses under Tab G. 3.2 Adherence to Mill Sampling SOPs The QA Manager review of Mill Personnel's adherence to the existing SOPs, confirmed that the QAJQC requirements established in the QAP and Chloroform QAP were met. 6 3.3 Analyte Completeness Review All analyses required by the GWDP for nitrate monitoring for the period were performed. 3.4 Data Validation The QAP and GWDP (August 24, 2012) identify the data validation steps and data QC checks required for the nitrate monitoring program. Consistent with these requirements, the QA Manager performed the following evaluations: a field data QA/QC evaluation, a holding time evaluation, an analytical method check, a reporting limit evaluation, a QC evaluation of sample duplicates, a QC evaluation of control limits for analysis and blanks, a receipt temperature evaluation, and a rinsate evaluation. Because no VOCs are analyzed for the nitrate contamination investigation, no trip blanks are required in the sampling program. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab H. 3.4.1 Field Data QA/QC Evaluation The QA Manager performs a review of all field recorded parameters to assess their adherence with QAP requirements. The assessment involved review of two sources of information: the Field Data Sheets and the Quatterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and stability of five parameters: conductance, pH, temperature, redox potential, and turbidity. Review of the Depth to Water data confirms that all depth measurements used for development of groundwater contour maps were conducted within a five-day period of each other. The results of this quarter's review are provided under Tab H. Based upon the review of the field data sheets, field work conformed with the QAP purging and field measurement requirements. A summary of the purging techniques employed and field measurements taken is described below: Purging Two Ca ing V:olum s with Stable Field Parameter (within 10% RPD) Wells TWN-01, TWN-04, and TWN-18 were sampled after two casing volumes were removed. Field parameters pH, specific conductivity, turbidity, water temperature, and redox potential were measured during purging. All field parameters for this requirement were stable within 10% RPD. Purging a WeU LoDryne. sand StabiUty of a Limited Li.l of Field Parameter Wells TWN-03 and TWN-07 were purged to dryness before two casing volumes were evacuated. After well recovery, one set of measurements for the field parameters of pH, specific conductivity, and water temperature only were taken; the samples were collected, and another set of measurements for pH, specific conductivity, and water temperature were taken. Stabilization of pH, conductivity and temperature are required within 10% RPD under the QAP. All field parameters for this requirement were stable within 10% RPD. Continuously Pumped Wells Wells TWN-02, TW4-22, TW4-24, and TW4-25 are continuously pumped wells. These wells are pumped on a set schedule per the remediation plan and are considered sufficiently evacuated to 7 immediately collect a sample. As previously noted, TW4-22, TW4-24, and TW4-25 are chloroform investigation wells and are sampled under the chloroform program. Data for nitrate and chloride are provided here for completeness purposes. During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water to the nearest 0.01 foot. All field parameters for all wells were within the QAP required limits, as indicated below. The review of the field sheets for compliance with QAP requirements resulted in the observations noted below. The QAP requirements in Attachment 2-3 specifically state that field parameters must be stabilized to within 10% over at least 2 consecutive measurements for wells purged to two casing volumes or to dryness. The QAP Attachment 2-3 states that turbidity should be less than 5 NTU prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP Attachment 2-3 does not require that turbidity measurements be less than 5 NTU prior to sampling. As such the noted observations regarding turbidity measurements greater than 5 NTU below are included for information purposes only. • Six well measurements exceeded the QAP' s 5 NTU turbidity goal as noted in Tab H. All required turbidity RPD's met the QAP Requirement to stabilize within 10%. EFRI's letter to DRC of March 26, 2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In response to DRC's subsequent correspQndence dated June 1, 2010 and June 24, 2010, EFRI completed a monitoring well redevelopment program. The redevelopment report was submitted to DRC on September 30, 2011. DRC responded to the redevelopment report via letter on November 15, 2012. Per the DRC letter dated November 15, 2012, the field data generated this quarter are compliant with the turbidity requirements of the approved QAP. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided in Tab H. All samples were received and analyzed within the required holding time. 3.4.3 Analytical Method Checklist All analytical methods reported by the laboratory were checked against the required methods enumerated in the QAP. Analytical method checks are provided in Tab H. All methods were consistent with the requirements of the QAP. 3.4.4 Reporting Limit Evaluation All analytical method reporting limits ("RLs") reported by the laboratory were checked against the reporting limits enumerated in the QAP. Reporting Limit Checks are provided in Tab H. All analytes were measured and reported to the required reporting limits, with the exception of several samples that had increased reporting limits due to matrix interference or required dilution due to the sample concentration. However, in all of those cases the analytical results were 8 greater than the reporting limit used. 3.4.5 QA/QC Evaluation for Sample Duplicates Section 9 .1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results are less than 5 times the required detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05- 01 as cited in the QAP. The RPDs are calculated for duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits. However, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPD is greater than 20%. The duplicate results were within a 20% RPD. Results of the RPD test are provided in Tab H. 3.4.6 Other Laboratory QA/QC Section 9.2 of the QAP requires that the laboratory's QA/QC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate Analytical Laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, EFRI' s QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided in Tab H. The lab QA/QC results met these specified acceptance limits. The QAP Section 8.1 .2 requires that a Matrix Spike/Matrix Spike Duplicate ("MS/MSD") pair be analyzed with each analytical batch. The QAP does not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the MS/MSD pair be prepared on EFRI samples only. Acceptance limits for MS/MSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the QAP requirement to analyze an MS/MSD pair with each analytical batch was met. While the QAP does not require it, the recoveries were reviewed for compliance with the laboratory established acceptance limits. The QAP does not require this level of review, and the results of this review are provided for information only. The information from the Laboratory QA/QC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for the samples were within acceptable laboratory limits for the regulated compounds except as indicated in Tab H. The two data recoveries that are outside the laboratory established acceptance limits do not affect the quality or usability of the data because the recoveries are above the acceptance limits and are indicative of matrix interference. Matrix interferences are applicable to the individual sample results only. The requirement in the 9 QAP to analyze a MS/MSD pair with each analytical batch was met and as such the data are compliant with the QAP. The information from the Laboratory QA/QC Summary Reports indicates that the Laboratory Control Sample recoveries were acceptable, which indicate that the analytical system was operating properly. The QAP Section 8.1.2 requires that each analytical batch shall be accompanied by a reagent blank. All analytical batches routinely contain a blank, which is a laboratory-grade water blank sample made and carried through all analytical steps. For the Mill samples, a method blank is prepared for all analytical methods. The information from the Laboratory QA/QC Summary Reports indicates that the method blanks did not contain detections of any target analytes above the Reporting Limit. 3.4.7 Receipt Temperature Evaluation Chain of Custody sheets were reviewed to confirm compliance with the QAP requirement in QAP Table 1 that samples be received at 6°C or lower. Sample temperatures checks are provided in Tab H. All samples were received within the required temperature limit. 3.4.8 Rinsate Check Rinsate checks are provided in Tab H. A comparison of the rinsate blank sample concentration levels to the QAP requirements -that rinsate sample concentrations be one order of magnitude lower than that of the actual well -indicated that all of the rinsate blank analytes met this criterion. AI rinsate and DIFB blank samples were non-detect for the quarter. 4.0 INTERPRETATIONOFDATA 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions. 4.1.1 Current Site Groundwater Contour Map As stated above, a listing of groundwater level readings for the current quarter (shown as depth to groundwater in feet) is included under Tab C. The data from this tab has been interpreted (kriged) and plotted in a water table contour map, provided under the same tab. The contour map is based on the current quarter's data for all wells. The water level contour map indicates that perched water flow ranges from generally southwesterly beneath the Mill site and tailings cells to generally southerly along the eastern and western margins of White Mesa. Perched water mounding associated with the wildlife ponds locally changes the generally southerly perched water flow patterns. For example, northeast of the Mill site, mounding associated with wildlife ponds results in locally northerly flow near PIEZ-1. The impact of the mounding associated with the northern ponds, to which water has not been delivered since March 2012, is diminishing and is expected to continue to diminish as the mound decays due to reduced recharge. 10 Not only has recharge from the wildlife ponds impacted perched water elevations and flow directions at the site, but the cessation of water delivery to the northern ponds, which are generally upgradient of the nitrate and chloroform plumes at the site, has resulted in changing conditions that are expected to impact constituent concentrations and migration rates within the plumes. Specifically, past recharge from the ponds has helped limit many constituent concentrations within the plumes by dilution while the associated groundwater mounding has increased hydraulic gradients and contributed to plume migration. Since use of the northern wildlife ponds ceased in March 2012, the reduction in recharge and decay of the associated groundwater mound are expected to increase many constituent concentrations within the plumes while reducing hydraulic gradients and acting to reduce rates of plume migration. EFRI and its consultants have raised the issues and potential effects associated with cessation of water delivery to the northern wildlife ponds during discussions with DRC in March 2012 and May 2013. The impacts associated with cessation of water delivery to the northern ponds are expected to propagate downgradient (south and southwest) over time. Wells close to the ponds are generally expected to be impacted sooner than wells farther downgradient of the ponds. Therefore, constituent concentrations are generally expected to increase in downgradient wells close to the ponds before increases are detected in wells farther downgradient of the ponds. Although such increases are anticipated to result from reduced dilution, the magnitude and timing of the increases are difficult to predict due to the complex permeability distribution at the site and factors such as pumping and the rate of decay of the groundwater mound. The potential exists for some wells completed in higher permeability materials to be impacted sooner than some wells completed in lower permeability materials even though the wells completed in lower permeability materials may be closer to the ponds. Localized increases in concentrations of constituents such as nitrate and chloride within and near the nitrate plume may occur even when the nitrate plume is under control based on the Nitrate CAP requirements. Ongoing mechanisms that can be expected to increase the concentrations of nitrate and chloride locally as a result of reduced wildlife pond recharge include but are not limited to: 1) Reduced dilution -the mixing of low constituent concentration pond recharge into existing perched groundwater will be reduced over time. 2) Reduced saturated thicknesses -dewatering of higher permeability layers recetvmg primarily low constituent concentration pond water will result in wells intercepting these layers receiving a smaller proportion of the low constituent concentration water. The combined impact of the above two mechanisms may be especially evident at chloroform pumping wells MW-4, MW-26, TW4-4, TW4-19, and TW4-20; nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2; and non-pumped wells adjacent to the pumped wells. The overall impact is expected to be generally higher constituent concentrations in these wells over the short term until mass reduction resulting from pumping and natural attenuation eventually reduce concentrations. In addition to changes in the flow regime caused by reduced wildlife pond recharge, perched flow directions are locally influenced by operation of the chloroform and nitrate pumping wells. 11 As shown in the detail water level map provided under Tab C, well defined cones of depression are evident in the vicinity of all chloroform pumping wells except TW 4-4, which began pumping in the first quarter of 2010. Although operation of chloroform pumping well TW 4-4 has depressed the water table in the vicinity of TW4-4, a well-defined cone of depression is not clearly evident. The lack of a well-defined cone of depression near TW4-4 likely results from 1) variable permeability conditions in the vicinity of TW4-4, and 2) persistent relatively low water levels at adjacent well TW4-14. As of the previous quarter, well-defined cones of depression were also not clearly evident near nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2, most likely because they had not had sufficient time to develop. Pumping of these wells began during the first quarter of 2013. Water level patterns near these wells are expected to be influenced by the presence of and the decay of the groundwater mound associated with the northern wildlife ponds, and by the persistently low water level elevation at TWN-7, which is located upgradient of the nitrate pumping wells. Although operation of the nitrate pumping system had not yet produced a well- defined impact on water levels, continued operation of the system was expected to produce a well-defined capture zone that would merge with and enhance the capture associated with the chloroform pumping system. During the current quarter, a large decrease in water level at nitrate pumping well TW4-25 has resulted in an apparently large cone of depression near that well. The large decrease in water level at TW4-25 combined with decreases at nitrate pumping wells TW4-22 and TW4-24, and adjacent chloroform pumping wells TW4-19 and TW4-20, has resulted in an apparently large increase in the combined influence of the nitrate and chloroform pumping systems. The long term interaction between nitrate and chloroform pumping systems will, however, require more data to be collected as part of routine monitoring. As discussed above, variable permeability conditions is one likely reason for the lack of a well- defined cone of depression near chloroform pumping well TW4-4. Changes in water levels at wells immediately south of TW4-4 resulting from TW4-4 pumping are expected to be muted because TW4-4 is located at a transition from relatively high to relatively low permeability conditions south (downgradient) of TW4-4. The permeability of the perched zone at TW4-6 and TW4-26, and recently installed wells TW4-29, TW4-30, TW4-31, TW4-33, and TW4-34, is one to two orders of magnitude lower than at TW4-4. Any drawdown of water levels at wells immediately south of TW4-4 resulting from TW4-4 pumping is also difficult to determine because of the general, long-term increase in water levels in this area due to recharge from the wildlife ponds. Water levels at TW4-4 and TW4-6 increased by nearly 2.7 and 2.9 feet, respectively, between the fourth quarter of 2007 and the fourth quarter of 2009 (just prior to the start of TW 4-4 pumping) at rates of approximately 1.2 feet/year and 1.3 feet/year, respectively. However, the increase in water level at TW4-6 has been reduced since the start of pumping at TW4-4 (first quarter of 2010) to approximately 0.5 feet/year suggesting that TW4-6 is within the hydraulic influence of TW4-4 (note: hydrographs for these wells are provided in the quarterly Chloroform Monitoring Report, EFRI 2013). Water level elevations at these wells are eventually expected to be influenced by cessation of water delivery to the northern wildlife ponds as discussed above. Recharge from the southern wildlife pond is expected to continue to have an effect on water 12 levels near TW 4-4, but the effects related to recharge from the northern ponds is expected to diminish over time as water is no longer delivered to the northern ponds. The lack of a well-defined cone of depression at TW 4-4 is also influenced by the persistent, relatively low water level at non-pumping well TW4-14, located east of TW4-4 and TW4-6. For the current quarter, the water level at TW4-14 (approximately 5528.2 feet above mean sea level ["ft amsl"]) is approximately 12 feet lower than the water level at TW4-6 (approximately 5539.9 ft amsl) and 15 feet lower than at TW4-4 (approximately 5543.3 ft amsl) even though TW4-4 is pumpmg. Well TW 4-27 (installed south of TW 4-14 in the fourth quarter of 2011) has a static water level of approximately 5527.1 ft amsl, similar to TW4-14 (approximately 5528.2 ft amsl). Prior to the installation of TW4-27, the persistently low water level at TW4-14 was considered anomalous because it appeared to be downgradient of all three wells TW4-4, TW4-6, and TW4-26, yet chloroform was not detected at TW4-14. Chloroform had apparently migrated from TW4-4 to TW4-6 and from TW4-6 to TW4-26 which suggested that TW4-26 was actually downgradient of TW4-6, and TW4-6 was actually downgradient of TW4-4, regardless of the flow direction implied by the low water level at TW4-14. The water level at TW4-26 (5538.97 feet amsl) is, however, lower than water levels at adjacent wells TW4-6 (5539.85 feet amsl), and TW4-23 (5542.96 feet amsl), as shown in the detail water level map under Tab C. Hydraulic tests indicate that the permeability at TW4-27 is an order of magnitude lower than at TW4-6 and three orders of magnitude lower than at TW4-4 (see Hydro Geo Chern, Inc. [HGC], September 20, 2010: Hydraulic Testing of TW4-4, TW4-6, and TW4-26, White Mesa Uranium Mill, July 2010; and HGC, November 28, 2011: Installation, Hydraulic Testing, and Perched Zone Hydrogeology of Perched Monitoring Well TW4-27, White Mesa Uranium Mill Near Blanding, Utah). The similar water levels at TW4-14 and TW4-27, and the low permeability estimate at TW4-27 suggest that both wells are completed in materials having lower permeability than nearby wells. The low permeability condition likely reduces the rate of long-term water level increase at TW4-14 and TW4-27 compared to nearby wells, yielding water levels that appear anomalously low. This behavior is consistent with hydraulic test data collected from recently installed wells TW4-29, TW4-30, TW4-31, TW4-33 and TW4-34 which indicate that the permeability of these wells is one to two orders of magnitude higher than the permeability of TW4-27 (see HGC, January 23, 2014; Contamination Investigation Report, TW4-12 and TW4- 27 Areas, White Mesa Uranium Mill Near Blanding, Utah). 4.1.2 Comparison of Current Groundwater Contour Map to Groundwater Contour Map for Previous Quarter The groundwater contour maps for the Mill site for the previous quarter, as submitted with the Nitrate Monitoring Report for the previous quarter, are attached under Tab D. A comparison of the water table contour maps for the current (fourth quarter of 2013) to the water table contour maps for the previous quarter (third quarter of 2013) indicates more pronounced drawdowns related to operation of chloroform pumping wells TW4-19 and TW4-20 and nitrate pumping well TW4-25. Nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2 were brought into operation during the first quarter of 2013 and their impact on water 13 level patterns was not clearly evident as of the previous quarter. During the current quarter (as will be discussed below and in Section 4.2.1 ), a large decrease in water level at nitrate pumping well TW4-25 has resulted in an apparently large cone of depression near that well. The large decrease in water level at TW4-25 combined with decreases at nitrate pumping wells TW4-22 and TW4-24, and adjacent chloroform pumping wells TW4-19 and TW4-20, has resulted in apparently large cones of depression associated with these wells. Otherwise, water levels and water level contours for the site have not changed significantly since the last quarter. As discussed in Section 4.1.1, pumping at chloroform well TW4-4, which began in the first quarter of 2010, has depressed the water table near TW4-4, but a well-defined cone of depression is not clearly evident, likely due to variable permeability conditions near TW 4-4 and the persistently low water level at adjacent well TW4-14. Reported decreases in water levels (increases in drawdown) of approximately 4 feet and 9 feet occurred in chloroform pumping wells TW4-19 and TW4-20, respectively. Furthermore, decreases of approximately 2 feet, 3 feet, and 25 feet occurred, respectively, in nitrate pumping wells TW4-22, TW4-24, and TW4-25. Changes in water levels at other pumping wells (chloroform pumping wells MW-4, MW-26 and TW4-4, and nitrate pumping well TWN-2) were less than 2 feet. Water level fluctuations at pumping wells typically occur in part because of fluctuations in pumping conditions just prior to and at the time the measurements are taken. A water level decrease of approximately 3 feet was reported at TW4-21. This decrease is likely the result of its location between pumping wells TW4-19 and TW4-25. The quarterly Chloroform Monitoring Report provides additional details on water levels in chloroform pumping wells. The decreases in water levels (increases in drawdown) at chloroform pumping wells TW4-19 and TW4-20 have increased the apparent capture of these wells relative to other pumping wells. The large cone of depression associated with nitrate pumping well TW4-25 has resulted in a relatively large zone of capture associated with this well. Furthermore, the apparent capture associated with TW4-25 has increased the apparent combined capture of chloroform pumping wells MW-26, TW4-19, and TW4-20 compared to last quarter. Water level decreases ranging from approximately 0.55 to 1.4 feet at Piezometers 1 and 2, and TWN-4, likely result from cessation of water delivery to the northern wildlife ponds as discussed in Section 4.1.1 and the consequent continuing decay of the associated perched water mound. The water level decrease of approximately 1.3 feet reported for TWN-1 is likely related to both decay of the perched water mound and operation of nitrate pumping well TW4-25. Water level decreases of nearly 5 feet at MW-3, of nearly 4 feet at MW-20, of approximately 6 feet at MW-23 and of approximately 5 feet at MW-37 were reported. These decreases are likely the result of purging and sampling these wells prior to measuring water levels. Because these wells have relatively low permeability, there was likely insufficient time for water levels to have fully recovered from purging prior to water level measurement. Although water was reported to be present at the bottom of piezometer DR-22 last quarter, DR-22 is reported to be dry this quarter. 14 4.1.3 Hydrographs Attached under Tab E are hydrographs showing groundwater elevation in each nitrate contaminant investigation monitor well over time. Per the CAP, nitrate wells TWN-6, TWN-14, TWN-16, and TWN-19 have been maintained for depth to groundwater monitoring only. These hydrographs are also included in Tab E. As noted in Section 2.1.1, nitrate wells TWN-05, TWN-08, TWN-09, TWN-10, TWN-11, TWN- 12, TWN-13, TWN-15, and TWN-17 were abandoned in accordance with the DRC-approved Well Abandonment Procedure on July 31, 2013. The historic hydrographs will not be included in future quarterly reports unless requested by DRC. 4.1.4 Depth to Groundwater Measured and Groundwater Elevation Attached in Tab F are tables showing depth to groundwater measured and groundwater elevation over time for each of the wells listed in Section 2.1.1 above. As noted in Section 2.1.1, nitrate wells TWN-05, TWN-08, TWN-09, TWN-10, TWN-11, TWN- 12, TWN-13, TWN-15, and TWN-17 were abandoned in accordance with the DRC-approved Well Abandonment Procedure on July 31, 2013. The historic measured depth to groundwater and groundwater elevation data will not be included in future quarterly reports unless requested byDRC. 4.2 Effectiveness of Hydraulic Containment and Capture 4.2.1 Hydraulic Containment and Control The CAP states that hydraulic containment and control will be evaluated in part based on water level data and in part on concentrations in wells downgradient of pumping wells TW4-22 and TW4-24. As per the CAP, the current quarter is the first quarter that hydraulic capture associated with nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2 will be evaluated Hydraulic containment and control based on water level data will be considered successful per the CAP if the entire nitrate plume upgradie~t of TW4-22 and TW4-24 falls within the combined capture of the nitrate pumping wells. Capture zones based on water level contours calculated by kriging the current quarter's water level data are provided on water level contour maps included under Tab C. The nitrate capture zones are defined by the bounding stream tubes associated with nitrate pumping wells. Each bounding stream tube represents a flow line parallel to the hydraulic gradient and therefore perpendicular to the intersected water level contours. Assuming that the stream tubes do not change over time, all flow between the bounding stream tubes associated with a particular pumping well is presumed to eventually reach and be removed by that well. Capture associated with chloroform pumping wells is also included on these maps because the influence of the chloroform and nitrate pumping systems overlap. The specific methodology for calculating the nitrate capture zones is substantially the same as that used since the fourth quarter of 2005 to calculate the capture zones for the chloroform 15 program, as agreed to by the DRC and International Uranium (USA) Corp. The procedure for calculating nitrate capture zones is as follows: 1) Calculate water level contours by gridding the water level data on approximately 50-foot centers using the ordinary linear kriging method in Surfer™. Default kriging parameters are used that include a linear variogram, an isotropic data search, and all the available water level data for the quarter, including relevant seep and spring elevations. 2) Calculate the capture zones by hand from the kriged water level contours following the rules for flow nets: -from each pumping well, reverse track the stream tubes that bound the capture zone of each well, -maintain perpedicularity between each stream tube and the kriged water level contours. Cones of depression associated with the nitrate pumping wells were not clearly evident as of last quarter, indicating that hydraulic containment of the portion of the nitrate plume upgradient of TW4-22 and TW4-24 had not yet been achieved. During the current quarter, decreases in water levels at nitrate pumping wells TW4-22 and TW4-24, and adjacent chloroform pumping wells TW4-19 and TW4-20, combined with the large water level decrease at nitrate pumping well TW4-25, have created apparently significant cones of depression and detectable capture associated with many of the nitrate pumping wells, in particular TW4-25. The apparent cone of depression at TW4-25 has expanded the apparent capture of the chloroform pumping system to the west. The resulting combined capture of both systems appears to encompass nearly half of the nitrate plume upgradient of TW4-22 and TW4-24. The actual proportion of the nitrate plume upgradient of TW4-22 and TW4-24 that is under hydraulic control at the present time is likely less than indicated by the capture zones displayed on the water level contour maps provided under Tab C. The apparent influence of TW4-25 is likely overestimated because of the large decline in water level measured in TW4-25 this quarter. The capture associated with nitrate pumping wells is, however, expected to increase over time as water levels continue to decline due to pumping and to cessation of water delivery to the northern wildlife ponds. Slow development of hydraulic capture is consistent with and expected based on the relatively low permeability of the perched zone at the site. Furthermore, the presence of the perched groundwater mound, and the apparently anomalously low water level at TWN-7, will influence the definition of capture associated with the nitrate pumping system. That pumping is likely sufficient to eventually capture the entire plume upgradient of TW4-22 and TW4-24 as can be demonstrated by comparing the combined average pumping rates of all nitrate pumping wells for the current quarter to estimates of pre-pumping flow through the nitrate plume near the locations of TW4-22 and TW4-24. The pre-pumping flow calculation is assumed to represent a steady state 'background' condition that includes constant recharge, hydraulic gradients, and saturated thicknesses. Changes after pumping are assumed to result only from pumping. As will be discussed below, the average combined nitrate pumping rate for the quarter exceeds the calculated pre-pumping rate of perched water flow through the nitrate plume by a factor between approximately 1.25 and 2.7. The cumulative volume of water removed by TW4-22, TW4-24, TW4-25, and TWN-2 during the current quarter was approximately 462,064 gallons. This equates to an average total 16 extraction rate of approximately 3.5 gpm over the 91 day quarter. This average accounts for time periods when pumps were off due to insufficient water columns in the wells. Pre-pumping flow through the nitrate plume near TW4-22 and TW4-24 was estimated using Darcy's Law to lie within a range of approximately 1.31 gpm to 2.79 gpm. Calculations were based on an average hydraulic conductivity range of 0.15 feet per day (ft/day) to 0.32 ft/day (depending on the calculation method), a pre-pumping hydraulic gradient of 0.025 feet per foot (ft/ft), a plume width of 1,200 feet, and a saturated thickness (at TW4-22 and TW4-24) of 56 feet. The hydraulic conductivity range was estimated by averaging the results obtained from slug test data that were collected automatically by data loggers from wells within the plume and analyzed using the KGS unconfined slug test solution available in Aqtesolve™ (see Hydro Geo Chern, Inc. [HGC], August 3, 2005: Perched Monitoring Well Installation and Testing at the White Mesa Uranium Mill, April Through June 2005; HGC, March 10, 2009: Perched Nitrate Monitoring Well Installation and Hydraulic Testing, White Mesa Uranium Mill; and HGC, March 17 2009: Letter Report to David Frydenlund, Esq, regarding installation and testing of TW4-23, TW4-24, and TW4-25) These results are summarized in Table 6. Data from fourth quarter 2012 were used to estimate the pre-pumping hydraulic gradient and saturated thickness. These data are also summarized in Tables 7 and 8. The average hydraulic conductivity was estimated to lie within a range of 0.15 ft/day to 0.32 ft/day. Averages were calculated four ways. As shown in Table 6 arithmetic and geometric averages for wells MW-30, MW-31, TW4-22, TW4-24, TW4-25, TWN-2, and TWN-3 were calculated as 0.22 and 0.15 ft/day, respectively. Arithmetic and geometric averages for a subset of these wells (MW-30, MW-31, TW4-22, and TW4-24) were calculated as 0.32 and 0.31 ft/day, respectively. The lowest value, 0.15 ft/day, represented the geometric average of the hydraulic conductivity estimates for all the plume wells. The highest value, 0.32 ft/day, represented the arithmetic average for the four plume wells having the highest hydraulic conductivity estimates (MW-30, MW-31, TW4-22, and TW4-24). Pre-pumping hydraulic gradients were estimated at two locations; between TW4-25 and MW-31 (estimated as 0.023 ft/ft), and between TWN-2 and MW-30 (estimated as 0.027 ft/ft). These results were averaged to yield the value used in the calculation (0.025 ft/ft). The pre-pumping saturated thickness of 56 feet was an average of pre-pumping saturated thicknesses at TW 4-22 and TW4-24. The hydraulic gradient and saturated thickness used in the calculations are assumed to represent a steady state 'background' condition. However, assumption of a steady state 'background' is inconsistent with the cessation of water delivery to the northern wildlife ponds, located upgradient of the nitrate plume. Hydraulic gradients and saturated thicknesses within the plume are declining as a result of two factors: reduced recharge from the ponds, and the effects of nitrate pumping. Separating the impacts of nitrate pumping from the impacts of reduced recharge from the ponds is problematic. Should pumping cease and 'background' conditions be allowed to re-establish, however, smaller hydraulic gradients and saturated thicknesses would be expected due to reduced recharge, which would lower estimates of 'background' flow. As a result, the 'background' flow calculated using the hydraulic gradient of 0.025 ft/ft and saturated thickness of 56 feet is considered conservatively large. Furthermore, using the 17 arithmetic average hydraulic conductivity of a subset of plume wells having the highest conductivities is considered less representative of actual conditions than using the geometric average conductivity of all of the plume wells. Nitrate pumping may therefore exceed flow through the plume by a factor greater than 2. 7, the high end of the calculated range. The CAP states that MW-5, MW-11, MW-30, and MW-31 are located downgradient ofTW4-22 and TW4-24. MW-30 and MW-31 are within the plume near its downgradient edge and MW-5 and MW -11 are outside and downgradient of the plume. Per the CAP, hydraulic control based on concentration data will be considered successful if the concentrations of nitrate in MW-30 and MW-31 remain stable or decline, and concentrations of nitrate in downgradient wells MW-5 and MW -11 do not exceed the 10 mg/L standard. Table 5 presents the nitrate concentration data for MW-30, MW-31, MW-5 and MW-11, which are down-gradient of pumping wells TW4-22 and TW4-24. Based on these concentration data, the nitrate plume is under control. The plume has not migrated downgradient to MW-5 or MW-11 because nitrate was not detected at MW-11 and was detected at a concentration less than 1 mg/L at MW-5. Between the previous and current quarters, nitrate concentrations increased slightly in both MW-30 and MW-31. Nitrate in MW-30 increased from 17.6 mg/L to 19.5 mg/L and nitrate in MW-31 increased from 21.7 mg/L to 23.9 mg/L. Changes in both wells were less than 20% suggesting the changes are within the range typical for sampling and analytical error. Although short-term fluctuations have occurred, nitrate concentrations in MW-30 and MW-31 have been relatively stable, demonstrating that plume migration is minimal or absent. Chloride has been relatively stable at MW-30 but appears to be increasing at MW-31 (see Tab J and Tab K, discussed in Section 4.2.4). The apparent increase in chloride and stable nitrate at MW-31 suggests a natural attenuation process that is affecting nitrate but not chloride. A likely process that would degrade nitrate but leave chloride unaffected is reduction of nitrate by pyrite. The likelihood of this process in the perched zone is discussed in HGC, December 7 2012; Investigation of Pyrite in the Perched Zone, White Mesa Uranium Mill Site, Blanding, Utah. 4.2.2 Current Nitrate and Chloride Isoconcentration Maps Included under Tab I of this Report are current nitrate and chloride iso-concentration maps for the Mill site. Nitrate iso-contours start at 5 mg/L and chloride iso-contours start at 100 mg/L because those values appear to separate the plumes from background. All nitrate and chloride data used to develop these iso-concentration maps are from the current quarter's sampling events. 4.2.3 Comparison of Areal Extent Although changes in concentration have occurred in wells within the nitrate plume, the boundaries of the plume have not changed significantly since the last quarter, except that the kriged plume boundary does not encompass well TW 4-18 as it did last quarter. The primary reason for this change is that the nitrate concentration at chloroform pumping well TW 4-19, located between the plume and TW4-18, decreased from approximately 18 mg/L to less than 5 mg/L. Nitrate concentrations at TW 4-18 have continued to increase, however, from 18 approximately 12 mg/L during the previous quarter to approximately 14 mg/L this quarter. Changes in this area are expected to result from changes in pumping and from the cessation of water delivery to the northern wildlife ponds. The reduction in low-nitrate recharge from the ponds appears to be having the anticipated effect of generally increased nitrate concentrations in wells downgradient of the ponds (see Tab 1 and Tab K, discussed in Section 4.2.4), which is the expected consequence of reduced dilution as discussed in Section 4.1.1. Although such increases in concentration have been anticipated as the result of reduced dilution, the magnitude and timing of the increases are difficult to predict due to the measured variations in hydraulic conductivity at the site and other factors. Regardless of the specific causes of the increase, nitrate at TW 4-18 is associated with the chloroform plume, is cross-gradient of the nitrate plume as defined in the CAP, and is within the capture zone of the chloroform pumping system (primarily chloroform pumping well MW-26). Perched water flow at TW4-18 is to the southwest in the same approximate direction as the main body of the nitrate plume. Nitrate concentrations at the downgradient edge of the plume (MW-30 and MW-31) continue to be relatively stable, demonstrating that plume migration is minimal or absent. With regard to chloroform, the boundary of the northern portion of the chloroform plume has moved slightly to the west toward nitrate pumping well TW4-24 since pumping began. More details regarding the chloroform data and interpretation are included in the Quarterly Chloroform Monitoring Report submitted under separate cover. 4.2.4 Nitrate and Chloride Concentration Trend Data and Graphs Attached under Tab 1 is a table summarizing values for nitrate and chloride for each well over time. Attached under Tab K are graphs showing nitrate and chloride concentration plots in each monitor well over time. As noted in Section 2.1.1, nitrate wells TWN-05, TWN-08, TWN-09, TWN-10, TWN-11, TWN- 12, TWN-13, TWN-15, and TWN-17 were abandoned in accordance with the DRC-approved Well Abandonment Procedure on July 31, 2013. The historic trend data will not be included in future quarterly reports unless requested by DRC. 4.2.5 Interpretation of Analytical Data Comparing the nitrate analytical results to those of the previous quarter, as summarized in the tables included under Tab 1, the following observations can be made for wells within and immediately surrounding the nitrate plume: a) Nitrate concentrations have increased by more than 20% in the following wells compared to last quarter: TW4-10, TW4-22, TWN-1 and TWN-2; b) Nitrate concentrations have decreased by more than 20% in the following wells compared to last quarter: MW-26 and TW4-19; 19 c) Nitrate concentrations have remained within 20% in the following wells compared to last quarter: MW-27, MW-30, MW-31, TW4-18, TW4-20, TW4-21, TW4-24, TW4-25, TWN-3, TWN-4, TWN-7, and TWN-18; d) MW-11, MW-25 and MW-32 remained non-detect; and e) TW4-16 increased from non-detect to 1.37 mg/L. As indicated, nitrate concentrations for 12 of the wells with detected nitrate were within 20% of the values reported for the wells during the previous quarter, suggesting that variations are within the range typical for sampling and analytical error. The remaining wells (MW-26, TW4-10, TW4-19, TW4-22, TWN-1, and TWN-2) had changes in concentration greater than 20%. Of the latter, MW-26 and TW4-19 are chloroform pumping wells, and TW4-22 and TWN-2 are nitrate pumping wells. TW4-10 is located adjacent to chloroform pumping well MW-26 and TWN-1 is located adjacent to nitrate pumping well TW4-25. Fluctuations in concentrations at pumping wells and wells adjacent to pumping wells likely result in part from the effects of pumping as discussed in Section 4.1.1. The change at TWN-1 from approximately 1.2 to 1.6 mg/L is also likely to result from 'noise' due to the low concentrations at this well. Nitrate pumping well TWN-2 had the highest detected nitrate concentration. Since the last quarter, the nitrate concentration in pumping well TWN-2 increased from approximately 80 mg/L to 111 mg/L. The nitrate concentration in nitrate pumping well TW4-22 increased from approximately 30 to 45 mg/L and chloroform increased from 9,640 1-1-g/L to 13,300 1-1-g/L. Chloroform changes are likely in response to the start-up of nitrate pumping in the first quarter and are affected by the presence of historically high chloroform concentrations at adjacent, cross- gradient well TW4-20. MW-27, located west ofTWN-2, and TWN-18, located north ofTWN-3, bound the nitrate plume to the west and north (See Figure I-1 under Tab I). In addition, the southernmost (downgradient) boundary of the plume remains between MW-30/MW-31 and MW-5/MW-11. Nitrate concentrations at MW-5 (adjacent to MW-11) and MW-11 have historically been low(< 1 mg/L) or non-detect for nitrate (See Table 5). MW-25, MW-26, MW- 32, TW4-16, TW4-5: TW4-25, TWN-1, and TWN-4 bound the nitrate plume to the east. As discussed above, TW4-18 is outside the kriged plume boundary this quarter (due to a decrease in concentration at TW4-19, located between the plume and TW4-18), although nitrate in well TW4-18 continues to increase (from approximately 12. to 14 mg/L between the previous and current quarters). The increases at TW4-18 (and other nearby wells) are likely the result of the cessation of water delivery to the northern wildlife ponds and the consequent decay of the associated groundwater mound. The reduction in low-nitrate recharge from the ponds appears to be having the anticipated effect of generally increasing nitrate concentrations in wells downgradient of the ponds as discussed in Section 4 .1.1. Nitrate concentrations outside the nitrate plume exceed 10 mg/L at a few locations: TW4-10 (16 mg/L), TW4-12 (16.4 mg/L), TW4-26 (15.9 mg/L), TW4-27 (29.8 mg/L), and TW4-28 (16.2 mg/L). All these wells are located southeast of the nitrate plume as defined in the CAP and all are separated from the plume by wells having nitrate concentrations that are either non-detect, or, if detected, are less than 10 mg/L. Concentrations at TW4-12 and TW4-27 are within 20% of their concentrations during the previous quarter. Increased nitrate at TW 4-10 most likely results from the same factors that resulted in the increases at TW4-18, primarily reduced dilution from 20 the northern wildlife ponds as discussed above. As with TW 4-18, nitrate at TW 4-10 is associated with the chloroform plume and is within the capture zone of the chloroform pumping system. Chloride concentrations are measured because elevated chloride (greater than 100 mg/L) is associated with the nitrate plume. Chloride concentrations at all measured locations are within 20% of their respective concentrations during the previous quarter except at the following locations: TW4-19 (decreased from 179 mg/L to 134 mg/L); and TW4-25 (decreased from 119 mg/L to 88.6 mg/L). TW4-19 is a chloroform pumping well; and TW4-25 is a nitrate pumping well. Fluctuations in concentrations at pumping wells and wells adjacent to pumping wells likely result in part from the effects of pumping. Future increases in concentrations at wells near the northern wildlife ponds are anticipated as a result of reduced dilution caused by cessation of water delivery to the northern wildlife ponds. 4.3 Estimation of Pumped Nitrate Mass and Residual Nitrate Mass within the Plume Nitrate mass removed by pumping is summarized in Table 2, and includes mass removed by both chloroform and nitrate pumping wells. Table 3 shows the volume of water pumped at each well and Table 4 provides the details of the nitrate removal for each well. Mass removal calculations begin with the third quarter of 2010 because the second quarter, 2010 data were specified to be used to establish a baseline mass for the nitrate plume. As stated in the CAP, the baseline mass is to be calculated using the second quarter, 2010 concentration and saturated thickness data "within the area of the kriged 10 mg/L plume boundary." The second quarter, 2010 data set was considered appropriate because "the second quarter, 2010 concentration peak at TWN-2 likely identifies a high concentration zone that still exists but has migrated away from the immediate vicinity of TWN-2." As shown in Table 2, a total of approximately 767 lb of nitrate has been removed from the perched zone since the third quarter of 2010. Prior to the current quarter, all direct nitrate mass removal resulted from operation of chloroform pumping wells MW-4, MW-26, TW4-4, TW4- 19, and TW4-20. During the current quarter: • A total of approximately 162 lb of nitrate was removed by the chloroform pumping wells and by nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2. • Of the 162 lb removed during the current quarter, approximately 137 lb, (or 85 %), was removed by the nitrate pumping wells. Baseline mass and current quarter mass estimates (nitrate+ nitrite as N) for the nitrate plume are approximately 43,700 lb and 41,150 lb, respectively. Mass estimates were calculated within the plume boundaries as defined by the kriged 10 mg/L isocon by 1) gridding (kriging) the nitrate concentration data on 50-foot centers; 2) calculating the volume of water in each grid cell based on the saturated thickness and assuming a porosity of 0.18; 3) calculating the mass of nitrate+nitrite as N in each cell based on the concentration and volume of water for each cell; and 4) totaling the mass of all grid cells within the 10 mg/L plume boundary. Data used in these calculations included data from wells listed in Table 3 of the CAP. The nitrate mass estimate for the current quarter is lower than the baseline estimate by 2,550 lb, and this difference is greater than the amount of nitrate mass removed directly by pumping. 21 Changes in the quarterly mass estimates are expected to result primarily from 1) nitrate mass removed directly by pumping, 2) natural attenuation of nitrate, and 3) changes in nitrate concentrations in wells within the plume as a result of re-distribution of nitrate within the plume and changes in saturated thicknesses. Redistribution of nitrate within the plume and changes in saturated thicknesses will be impacted by changes in pumping and in background conditions such as the decay of the perched water mound associated with the northern wildlife ponds. Cessation of water delivery to the northern wildlife ponds is expected to result in reduced saturated thicknesses and reduced dilution, which in turn is expected to result in increases in concentrations. The mass estimate during the current quarter (41,150 lb) was larger than the mass estimate during the previous quarter (36,930 lb) by 4,220 lb, or approximately 11 %. The primary reason for this difference is higher nitrate concentrations measured in many wells within the plume this quarter compared to last quarter especially TWN-2, which increased from approximately 80 to 111 mg/L. Increases are likely to result primarily from the cessation of water delivery to the northern wildlife ponds and the consequent decay of the associated groundwater mound. The reduction in low-nitrate recharge from the ponds appears to be having the anticipated effect of increasing nitrate concentrations in wells downgradient of the ponds. The impact of reduced dilution, which increases both concentrations and the calculated mass is not completely offset by reductions in saturated thicknesses (resulting from pumping and groundwater mound decay), which reduce both the calculated plume volume and calculated mass. Nitrate mass removal by pumping and natural attenuation (expected to result primarily from pyrite oxidation/nitrate reduction) act to lower nitrate mass within the plume. Changes resulting from redistribution of nitrate within the plume are expected to result in both increases and decreases in concentrations at wells within the plume and therefore increases and decreases in mass estimates based on those concentrations, thus generating 'noise' in the mass estimates. Furthermore, because the sum of sampling and analytical error is typically about 20%, changes in the mass estimates from quarter to quarter of up to 20% could result from typical sampling and analytical error alone. Only longer-term analyses of the mass estimates that minimize the impacts of these quarter to quarter variations will provide useful information on plume mass trends. Over the long term, nitrate mass estimates are expected to trend downward as a result of direct removal by pumping and through natural attenuation. As specified in the CAP, once eight quarters of data have been collected (struting with the first quarter of 2013), a regression trend line will be applied to the quarterly mass estimates and evaluated. The trend line will then be updated quarterly and reevaluated as additional quarters of data are collected. The evaluation will determine whether the mass estimates are increasing, decreasing, or stable. 22 5.0 LONG TERM PUMP TEST AT TWN-02, TW4-22, TW4-24, and TW4- 25 OPERATIONS REPORT 5.1 Introduction Beginning in January 2013, EFRI began long term pumping of TW4-22, TW4-24, TW4-25, and TWN-02 as required by the Nitrate CAP, dated May 7, 2012 and the SCO dated December 12, 2012. In addition, as a part of the investigation of chloroform contamination at the Mill site, EFRI has been conducting a Long Term Pump Test on MW-4, TW4-19, MW-26, and TW4-20, and, since January 31, 2010, TW4-4. The purpose of the test is to serve as an interim action that will remove a significant amount of chloroform-contaminated water while gathering additional data on hydraulic properties in the area of investigation. Because wells MW-4, TW4-19, MW-26, TW4-4 and TW4-20 are pumping wells that may impact the removal of nitrate, they are included in this report and any nitrate removal realized as part of this pumping is calculated and included in the quarterly reports. The following information documents the operational activities during the quruter. 5.2 Pumping Well Data Collection Data collected during the quarter included the following: • Measurement of water levels at MW-4, TW4-19, MW-26, and TW4-20 and, commencing regularly on March 1, 2010, TW4-4, on a weekly basis, and at selected temporary wells and permanent monitoring wells on a monthly basis. • Measurement of pumping history, including: pumping rates total pumped volume operational and non-operational periods. • Periodic sampling of pumped water for chloroform and nitrate/nitrite analysis and other constituents • Measurement of water levels weekly at TW4-22, TW4-24, TW4-25, and TWN-02 commencing January 28, 2013, and on a monthly basis selected temporary wells and permanent monitoring wells. 5.3 Water Level Measurements Beginning August 16, 2003, water level measurements from chloroform pumping wells MW-4, MW-26, and TW4-19 were conducted weekly. From commencement of pumping TW4-20, and regularly after March 1, 2010 for TW4-4, water levels in these two chloroform pumping wells have been measured weekly. From commencement of pumping in January 2013, water levels in wells TW4-22, TW4-24, TW4-25, and TWN-02 have been measured weekly. Copies of the weekly Depth to Water monitoring sheets for MW-4, MW-26, TW4-19, TW4-20, TW4-4, TW4- 22, TW4-24, TW4-25 and TWN-02 are included under Tab C. 23 Monthly depth to water monitoring is required for all of the chloroform contaminant investigation wells and non-pumping wells MW-27, MW-30, MW-31, TW4-21, TWN-1, TWN- 3, TWN-4, TWN-7, and TWN-18. Copies of the monthly depth to Water monitoring sheets are included under Tab C. 5.4 Pumping Rates and Volumes The pumping wells do not pump continuously, but are on a delay device. The wells purge for a set amount of time and then shut off to allow the well to recharge. Water from the pumping wells is either transferred to the Cell 1 evaporation pond or is used in the Mill process. The pumped wells are fitted with a flow meter which records the volume of water pumped from the well in gallons. The flow meter readings shown in Tab C are used to calculate the gallons of water pumped from the wells each quarter as required by Section 7 .2.2 of the CAP. The average pumping rates and quarterly volumes for each of the pumping wells are shown in Table 3. The cumulative volume of water pumped from each of the wells is shown in Table 4. No operational problems were observed with the wells or pumping equipment during the quarter. 6.0 CORRECTIVE ACTION REPORT There are no corrective actions resulting from the 4th quarter 2013 nitrate sampling event. 6.1 Assessment of Previous Quarter's Corrective Actions There were no corrective actions in the 3rd quarter 2013 nitrate sampling event. 7.0 CONCLUSIONS AND RECOMMENDATIONS As per the CAP, the current quarter is the first quarter that hydraulic capture associated with nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2 was evaluated. Capture zones were based on water level contours calculated by kriging the current quarter's water level data. The nitrate capture zones are defined by the bounding stream tubes associated with nitrate pumping wells (as shown in maps under Tab C). Each bounding stream tube represents a flow line parallel to the hydraulic gradient and therefore perpendicular to the intersected water level contours. Assuming that the stream tubes do not change over time, all flow between the bounding stream tubes associated with a particular pumping well is presumed to eventually reach and be removed by that well. Cones of depression associated with the nitrate pumping wells were not clearly evident as of last quarter, indicating that hydraulic containment of the portion of the nitrate plume upgradient of TW4-22 and TW4-24 had not yet been achieved. During the current quarter, decreases in water levels at nitrate pumping wells TW4-22 and TW4-24, and adjacent chloroform pumping wells TW4-19 and TW4-20, combined with a large water level decrease at nitrate pumping well TW4- 25, have created apparently significant cones of depression and detectable capture associated with many of the nitrate pumping wells, in particular TW4-25. The apparent cone of depression 24 at TW4-25 has expanded the apparent capture of the chloroform pumping system to the west. The resulting combined capture of both systems appears to encompass nearly half of the nitrate plume upgradient ofTW4-22 and TW4-24. The actual proportion of the nitrate plume upgradient of TW4-22 and TW4-24 that is under hydraulic control at the present time is likely less than indicated by the capture zones displayed on the water level contour maps (provided under Tab C). The influence of TW4-25 is likely overestimated because of the large decline in water level measured in TW 4-25 this quarter. The capture associated with nitrate pumping wells is, however, expected to increase over time as water levels continue to decline due to pumping and to cessation of water delivery to the northern wildlife ponds. Furthermore, the evaluation of the long term interaction between nitrate and chloroform pumping systems will require more data to be collected as part of routine monitoring. Slow development of hydraulic capture by the nitrate pumping system is consistent with, and expected based on the relatively low permeability of the perched zone at the site. Definition of capture associated with the nitrate pumping system will also be influenced by the perched groundwater mound and the apparently anomalously low water level at TWN-7. Current pumping is likely sufficient to eventually capture the entire nitrate plume upgradient of TW4-22 and TW4-24 as demonstrated by comparing the combined average pumping rates of all the nitrate pumping wells for the current quarter (approximately 3.5 gpm) to estimates of pre- pumping ('background') flow through the nitrate plume near the locations ofTW4-22 and TW4- 24 (calculated to lie between 1.31 gpm and 2.79 gpm). Calculations indicate that pumping during the current quarter exceeds the estimated pre-pumping rate of perched water flow through the nitrate plume by a factor between approximately 1.25 and 2.7, depending on the method used to calculate the average hydraulic conductivity within the plume. Because the pre-pumping flow calculations likely overestimate the new 'background' conditions caused by reduced recharge from the northern wildlife ponds, and because the average plume hydraulic conductivity estimate from the low end of the calculated range is likely to be more representative of actual conditions, nitrate pumping may exceed flow through the plume by a factor greater than 2.7. Fourth quarter, 2013 nitrate concentrations at many of the wells within and adjacent to the nitrate plume were within 20% of the values reported during the previous quarter, suggesting that variations are within the range typical for sampling and analytical error. Changes in concentration greater than 20% occurred in wells MW-26, TW4-10, TW4-19, TW4-22, TWN-1, and TWN-2. The concentrations in wells MW-11, MW-25 and MW-32 remained non-detect while the concentration in TW4-16 increased from non-detect to 1.37 mg/L. Of the wells showing changes in concentration greater than 20%, MW-26 and TW4-19 are chloroform pumping wells, and TW4-22 and TWN-2 are nitrate pumping wells. TW4-10 is located adjacent to chloroform pumping well MW-26 and TWN-1 is located adjacent to nitrate pumping well TW4-25. Fluctuations in concentrations at pumping wells and wells adjacent to pumping wells likely result in part from the effects of pumping. The change at TWN-1 from approximately 1.2 to 1.6 mg/L likely results from 'noise' due to the low concentrations at this well. The highest nitrate concentration (111 mg!L) was detected at nitrate pumping well TWN-2. Since the last quarter, the nitrate concentration in TWN-2 increased from approximately 80 mg/L 25 to 111 mg/L. The nitrate concentration in nitrate pumping well TW4-22 increased from approximately 30 to 45 mg/L and chloroform increased from 9,640 flg/L to 13,300 flg/L causing the boundary of the northern portion of the chloroform plume to move slightly to the west toward nitrate pumping well TW4-24. Chloroform changes are likely in response to the start-up of nitrate pumping in the first quarter and are affected by the presence of historically high chloroform concentrations at adjacent, cross-gradient well TW4-20. As discussed in Section 4.2.5, TW4-18 is again outside the kriged plume boundary due to a decrease in concentration at TW 4-19 (located between the plume and TW 4-18) between the previous and current quarters. Nitrate at TW4-18 continues to increase (from approximately 12 to 14 mg/L between the previous and current quarters). The increases at TW4-18 (and other nearby wells) are likely due to the cessation of water delivery to the northern wildlife ponds and the consequent decay of the associated groundwater mound. The reduction in low-nitrate recharge from the ponds appears to be having the anticipated effect of generally increased nitrate concentrations in wells downgradient of the ponds. Although such increases have been anticipated as the result of reduced dilution, the magnitude and timing of the increases are difficult to predict due to the measured variations in hydraulic conductivity at the site and other factors. Regardless of the specific causes of the increase, nitrate at TW 4-18 is associated with the chloroform plume, is cross-gradient of the nitrate plume as defined in the CAP, and is within the capture zone of the chloroform pumping system (primarily chloroform pumping well MW-26). Perched water flow at TW4-18 is to the southwest in the same approximate direction as the main body of the nitrate plume. Except in the immediate vicinity of TW4-18, the boundaries of the nitrate plume have not changed significantly since the last quarter, even though the plume is influenced by reduced dilution, by nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2, and changes in concentrations in wells within the plume. Well MW-27, located west of TWN-2, and TWN-18, located north of TWN-3, bound the nitrate plume to the west and north. In addition, the southernmost (downgradient) boundary of the plume remains between MW-30/MW-31 and MW-5/MW-11. Nitrate concentrations at MW-5 (adjacent to MW-11) and MW-11 have historically been low (< 1 mg/L) or non-detect for nitrate. Wells MW-25, MW-26, MW-32, TW4-16, TW4-5, TW4-25, TWN-1, and TWN-4 bound the nitrate plume to the east. Nitrate concentrations at MW-30 and MW-31 continue to be relatively stable, suggesting that plume migration is minimal or absent. Nitrate in MW-30 increased from 17.6 mg/L to 19.5 mg/L and nitrate in MW-31 increased from 21.7 mg/L to 23.9 mg/L. Changes in both wells were less than 20% suggesting the changes are within the range typical for sampling and analytical error. Based on the concentration data at MW-5, MW-11, MW-30, and MW-31, the nitrate plume is under control Chloride has been relatively stable at MW-30 but appears to be increasing at MW-31. The apparent increase in chloride and stable nitrate at MW -31 suggests a natural attenuation process that is affecting nitrate but not chloride. A likely process that would degrade nitrate but leave chloride unaffected is reduction of nitrate by pyrite. The likelihood of this process in the perched zone is discussed in HGC, December 7 2012; Investigation of Pyrite in the Perched Zone, White Mesa Uranium Mill Site, Blanding, Utah. 26 The baseline nitrate (nitrate+nitrite as N) plume mass calculated as specified in the CAP (based on second quarter, 2010 data) was approximately 43,700 lb. The nitrate plume mass estimate for the current quarter was calculated as 41,150 lb, which was higher than the previous quarter's estimate of 36,930 lb by 4,220 lb or 11 %. The primary reason for this difference is higher nitrate concentrations measured in many wells within the plume this quarter compared to last quarter, especially TWN-2, which increased from approximately 80 to 111 mg/L. Increases are likely due to the cessation of water delivery to the northern wildlife ponds and the consequent decay of the associated groundwater mound. The reduction in low-nitrate recharge from the ponds appears to be having the anticipated effect of increasing nitrate concentrations in wells downgradient of the ponds. The impact of reduced dilution, which increases both concentrations and the calculated mass is not completely offset by reductions in saturated thicknesses (resulting from pumping and groundwater mound decay), which reduce both the calculated plume volume and calculated mass. Nitrate mass removal by pumping and natural attenuation (expected to result primarily from pyrite oxidation/nitrate reduction) act to lower nitrate mass within the plume. Changes resulting from redistribution of nitrate within the plume are expected to result in both increases and decreases in concentrations at wells within the plume and therefore increases and decreases in mass estimates based on those concentrations, thus generating 'noise' in the mass estimates. Furthermore, because the sum of sampling and analytical error is typically about 20%, changes in the mass estimates from quarter to quarter of up to 20% could result from typical sampling and analytical error alone. Only longer-term analyses of the mass estimates that minimize the impact of these quarter to quarter variations will provide useful information on plume mass trends. Over the long term, nitrate mass estimates are expected to trend downward as a result of direct removal by pumping and through natural attenuation. As specified in the CAP, once eight quarters of data have been collected (starting with the first quarter of 2013), a regression trend line will be applied to the quarterly mass estimates and evaluated. The trend line will then be updated quarterly and reevaluated as additional quarters of data are collected. The evaluation will determine whether the mass estimates are increasing, decreasing, or stable. During the current quarter, a total of approximately 162 lb of nitrate was removed by the chloroform pumping wells and by nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN- 2. Of the 162 lb removed during the current quarter, approximately 137 lb, (or 85 %), was removed by the nitrate pumping wells. Nitrate concentrations outside the nitrate plume exceed 10 mg/L at a few locations: TW4-10 (16 mg/L), TW4-12 (16.4 mg/L), TW4-26 (15.9 mg/L), TW4-27 (29.8 mg/L), and TW4-28 (16.2 mg/L). All these wells are located southeast of the nitrate plume as defined in the CAP and all are separated from the plume by wells having nitrate concentrations that are either non-detect, or, if detected, are less than 10 mg/L. Concentrations at TW4-12 and TW4-27 are within 20% of their concentrations during the previous quarter. Increases at TW4-10 most likely result from the same factors that resulted in the increases at TW4-18, primarily reduced dilution from the northern wildlife ponds as discussed above. As with TW 4-18, nitrate at TW 4-10 is associated with the chloroform plume and is within the capture zone of the chloroform pumping system. 27 Chloride concentrations are measured because elevated chloride (greater than 100 mg!L) is associated with the nitrate plume. Chloride concentrations at all measured locations are within 20% of their respective concentrations during the previous quarter except at the following locations: TW4-19 (decreased from 179 mg!L to 134 mg/L); and TW4-25 (decreased from 119 mg/L to 88.6 mg/L). TW4-19 is a chloroform pumping well; and TW4-25 is a nitrate pumping well. Fluctuations in concentrations at pumping wells and wells adjacent to pumping wells likely result in part from the effects of pumping. Nitrate mass removal from the perched zone increased substantially by the start-up of nitrate pumping wells TW4-22, TW4-24, TW4-25, and TWN-2 during the first quarter. Continued operation of these wells is therefore recommended. Pumping these wells, regardless of any short term fluctuations in concentrations detected at the wells, helps to reduce downgradient nitrate migration by removing nitrate mass and reducing average hydraulic gradients, thereby allowing natural attenuation to be more effective. Continued operation of the nitrate pumping system is expected to eventually reduce nitrate concentrations within the plume and to further reduce or halt downgradient nitrate migration. Concentration trends are affected by the cessation of water delivery to the northern wildlife ponds which appears to be having the anticipated impact of reduced dilution (which is increasing constituent concentrations at some wells) and reduced hydraulic gradients (which will act in concert with pumping to reduce hydraulic gradients and reduce plume migration). While past recharge from the ponds has helped limit many constituent concentrations within the chloroform and nitrate plumes by dilution, the associated groundwater mounding has increased hydraulic gradients and contributed to plume migration. Since use of the northern wildlife ponds ceased in March 2012, the reduction in recharge and decay of the associated groundwater mound is expected to increase many constituent concentrations within the plumes while reducing hydraulic gradients and rates of plume migration. EFRI and its consultants have raised the issues and potential effects associated with cessation of water delivery to the northern wildlife ponds during discussions with DRC in March 2012 and May 2013. The impacts associated with cessation of water delivery to the northern ponds are expected to propagate downgradient (south and southwest) over time. Wells close to the ponds are generally expected to be impacted sooner than wells farther downgradient of the ponds. Therefore, constituent concentrations are generally expected to increase in downgradient wells close to the ponds before increases are detected in wells farther downgradient of the ponds. Although such increases are anticipated to result from reduced dilution, the magnitude and timing of the increases are difficult to predict due to the complex permeability distribution at the site and factors such as pumping and the rate of decay of the groundwater mound. The potential exists for some wells completed in higher permeability materials to be impacted sooner than some wells completed in lower permeability materials even though the wells completed in lower permeability materials may be closer to the ponds. Localized increases in concentrations of constituents such as nitrate and chloride within and near the nitrate plume may occur even when the nitrate plume is under control based on the Nitrate CAP requirements. Ongoing mechanisms that can be expected to increase the concentrations of nitrate and chloride locally as a result of reduced wildlife pond recharge include but are not limited to: 28 1) Reduced dilution -the mixing of low constituent concentration pond recharge into existing perched groundwater will be reduced over time. 2) Reduced saturated thicknesses -dewatering of higher permeability layers receiVmg primarily low constituent concentration pond water will result in wells intercepting these layers receiving a smaller proportion of the low constituent concentration water. The combined impact of the above two mechanisms may be especially evident at chloroform and nitrate pumping wells and non-pumped wells adjacent to the pumped wells. The overall impact is expected to be generally higher constituent concentrations in these wells over time until mass reduction resulting from pumping and natural attenuation eventually reduce concentrations. 8.0 ELECTRONIC DATA FILES AND FORMAT EFRI has provided to the Director an electronic copy of all laboratory results for groundwater quality monitoring conducted under the nitrate contaminant investigation during the Quarter, in Comma Separated Values ("CSV") format. A copy of the transmittal e-mail is included under Tab L. 29 9.0 SIGNATURE AND CERTIFICATION This document was prepared by Energy Fuels Resources (USA) Inc. on February 21, 2014. Energy Fuels Resources (USA) Inc. By: Frank Filas, P.E Vice President, Permitting and Environmental Affairs 30 Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including~d imprisonment for knowing violations. Frank Filas, P.E Vice President, Permitting and Environmental Affairs Energy Fuels Resources (USA) Inc. 31 Tables Table 1 Summary of Well Sampling and Constituents for the Period " WeD 1 ~~aruple Colle~tiQn, D3te1 Piezometer 01 10/16/2013 Piezometer 02 10116/2013 Piezometer 03 10/16/2013 TWN-01 10/16/2013 TWN~02 10/16/2013 TWN-03 10/17/2013 TWN-04 10/16/2013 TWN-07 10/16/2013 TWN-07R 10/15/2013 TWN-18 10/16/2013 TW4-22 10/29/2013 TW4-24 10/29/2013 TW4-25 10/29/2013 TWN-60 10117/2013 TW4-60 11114/2013 TWN-65 10/16/2013 Note: All wells were sampled for Nitrate and Chloride. TWN-60 is a DI Field Blank. TWN-65 is a duplicate of TWN-01. TW4-60 is the chloroform program DI Field Blank. Cominuously pumped well. Da~of~Lab ReiJort' 10/30/2013 10/30/2013 10/30/2013 10/30/2013 10/30/2013 10/30/2013 10/30/2013 10/30/2013 10/30/2013 10/30/2013 11/7/2013 11/7/2013 unno13 10/30/2013 11/26/2013 10/30/2013 Table 2 Nitrate Mass Removal Per Well Per Quarter MW-4 TW4-19 TW4-20 TW4-4 TW4-22 TW4-24 TW4-25 TWN-02 Quarter Totals I'' Quarter (lbs.) MW-26 (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) (lbs.) Q3 2010 3.2 0.3 5.8 1.7 4.7 NA NA NA NA 15.7 Q4 2010 3.8 0.4 17.3 1.4 5.1 NA NA NA NA 28.0 Ql 2011 2.9 0.2 64.5 1.4 4.3 NA NA NA NA 73.3 Q2 2011 3.5 0.1 15.9 2.7 4.7 NA NA NA NA 27.0 Q3 2011 3.5 0.5 3.5 3.9 5.4 NA NA NA NA 16.8 Q4 2011 3.8 0.8 6.2 2.5 6.4 NA NA NA NA 19.7 Q1 2012 3.6 0.4 0.7 5.0 6.0 NA NA NA NA 15.9 Q2 2012 3.7 0.6 3.4 2.1 5.2 NA NA NA NA 15.0 Q3 2012 3.8 0.5 3.6 2.0 4.7 NA NA NA NA 14.7 Q4 2012 3.2 0.4 5.4 1.8 4.2 NA NA NA NA 14.9 Q1 2013 2.5 0.4 14.1 1.4 3.6 8.1 43.4 7.5 14.8 95.7 Q2 2013 2.5 0.5 5.6 1.7 3.5 10.7 37.1 6.4 23.9 91.7 Q3 2013 3.0 0.4 48.4 1.4 3.8 6.3 72.8 6.9 33.4 176.5 Q4 2013 3.1 0.3 15.8 1.6 3.9 9.4 75.2 6.4 46.3 162.1 Well Totals (pounds) 46.1 5.9 210.2 30.6 65.5 34.5 228.5 27.3 118.4 767.0 Table 3 Nitrate Well Pumping Rates and Volumes Volume of Water Pumped Pumping Well Name During the Quarter (gals) Average Pump Rate (gpm) MW-4 70,340.4 4.3 MW-26 24,207.6 10.3 TW4-4 60,233.6 7.8 TW4-19 403,974.0 14.0 TW4-20 19,280.2 9.9 TW4-22 24,952.2 18.2 TW4-24 260,555.3 17.8 TW4-25 126,576.5 18 TWN-2 49,979.9 18.3 Table4 Table 4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped I' MW-4 MW-26 ' I I Total Total Total Pumped Total Total Total Pumped Cone Cone Pumped Total Total Quarter Pumped (gal) Conc(mg/L) Cone (ug/L) (liters) Total (ug) (grams) (pounds) (gal) (mg/L) (ug/L) (liters) Total (ug) (grams) (pounds) Total Gallons pumped for Total the quarter Total pumped Total grams/453. I Calculations from the Concentration Concentration gallons/3.785 Concentration ug/1000000 592 to and Data Flow Meter from the in mg/LX1 000 to to conver to in ug/L X total to convert to convert to Origination data analytical data convert to ug/L liters liters grams pounds 03 2010 79859.1 4.8 4800 302266.7 1450880129 1450.9 3.20 63850.0 0.6 600 241672.3 145003350 145 0.32 04 2010 90042.2 5 5000 340809.7 1704048635 1704.0 3.76 60180.0 0.7 700 227781.3 159446910 159 0.35 012011 76247.6 4.6 4600 288597.2 1327546964 1327.5 2.93 55130.0 0.5 500 208667,1 104333525 104 0.23 02 2011 85849.3 4.9 4900 324939.6 1592204042 1592.2 3.51 55800.6 0.3 300 211205.3 63361581 63 0.14 03 2011 85327.7 4.9 4900 322965.3 1582530188 1582.5 3.49 65618.0 0.9 900 248364.1 223527717 224 0.49 I 04 2011 89735.0 5.1 5100 339647.0 1732199573 1732.2 3.82 50191,3 2 2000 189974,1 379948141 380 0.84 012012 90376.4 4.8 4800 342074.7 1641958435 1642.0 3.62 31440.1 1.7 1700 119000.8 202301323 202 0.45 I 02 2012 90916,5 4.9 4900 344118.8 1686181940 1686.2 3.72 26701.2 2.5 2500 101064.1 252660294 253 0.56 Q3 2012 91607.0 5 5000 346732.5 1733662475 1733.7 3.82 25246.0 2.6 2600 95556.1 248445886 248 0.55 04 2012 78840.0 4.8 4800 298409.4 1432365120 1432.4 3.16 30797.0 1.46 1460 116566.6 170187302 170 0.38 012013 62943.7 4.78 4780 238241.9 1138796304 1138.8 2.51 22650.7 2.27 2270 85732.9 194613682 195 0.43 I 02 2013 71187.3 4.22 4220 269443.9 1137053387 1137.1 2.51 25343.4 2.11 2110 95924.8 202401263 202 0.45 03 2013 72898.8 4.89 4890 275922.0 1349258375 1349.3 2.97 25763.0 1.98 1980 97513.0 193075651 193 0.43 Q42013 70340.4 5.25 5250 266238.4 1397751674 1397.8 3.08 24207.6 1.38 1380 91625.8 126443557 126 0.28 Totals Since Q3 2010 1136170.95 46.09 562918.9 5.88 Highlighted cells are the total for the current quarter Table4 Table 4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped TW4-19 TW4-20 I l : I' I !Total Pumpecj Cone Cone Total Pumped Total Total Total Pumped Cone Cone Total Pumped Total Total Quarter (gal) (mg/L) (ug/L) (liters) Total (ug) (grams) (pounds) (gal) (mg/L) (ug/L) (liters) Total (ug) (grams) (pounds) I I I Calculations I and Data I Origination 03 2010 116899.2 5.9 5900 442463.5 2.611E+09 2611 5.76 39098.3 5.3 5300 147987.1 784331447 784 1.73 Q4 2010 767970.5 2.7 2700 2906768.3 7.848E+09 7848 17.30 36752.5 4.6 4600 139108.2 639897778 640 1.41 012011 454607.9 17 17000 1720690.9 2.925E+10 29252 64.49 37187.5 4.4 4400 140754.7 619320625 619 1.37 I Q2 2011 159238.9 12 12000 602719.2 7.233E+09 7233 15.95 67907.7 4.8 4800 257030.6 1.234E+09 1234 2.72 I Q3 2011 141542.6 3 3000 535738.7 1.607E+09 1607 3.54 72311.2 6.5 6500 273697.9 1.779E+09 1779 3.92 I Q4 2011 147647.2 5 5000 558844,7 2.794E+09 2794 6.16 72089.3 4.2 4200 272858.0 1.146E+09 1146 2.53 012012 148747.0 0.6 600 563007.4 337804437 338 0.74 76306.0 7.9 7900 288818.2 2.282E+09 2282 5.03 Q2 2012 172082.0 2.4 2400 651330.5 1.563E+09 1563 3.45 22956.4 11 11000 86890.1 955790963 956 2.11 I 03 2012 171345.0 2.5 2500 648540.8 1.621E+09 1621 3.57 22025.0 10.8 10800 83364.6 900337950 900 1.98 i Q4 2012 156653.0 4.1 4100 592931.6 2.431E+09 2431 5.36 20114.0 11 11000 76131.5 837446390 837 1.85 012013 210908.0 7.99 7990 798286.8 6.378E+09 6378 14.06 18177.0 9.07 9070 68799.9 624015501 624 1.38 I Q2 2013 226224.0 2.95 2950 856257.8 2.526E+09 2526 5.57 20252.4 9.76 9760 76655.3 748156060 748 1.65 Q3 2013 329460.1 17.6 17600 1247006.5 2.195E+10 21947 48.39 19731.0 8.65 8650 74681.8 645997873 646 1.42 Q42013 403974.0 4.7 4700 1529041.6 7.186E+09 7186 15.84 19280.2 9.64 9640 72975.6 703484369 703 1.55 Totals Since Q3 2010 3607299.4 210.18 544188.5 30.64 Highlighted cells are the total for the current quarter Table 4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped TW4-4 TW4-22 " I r Total Total Total Total Pumped Cone Cone Pumped Total Total Pumped Cone Cone Pumped Total Total Quarter (gal) (mg/L) (ug/L) (liters) Total (ug) (grams) (pounds) (gal) (mg/L) (ug/L) (liters) Total (ug) (grams) (pounds) I I I Calculations I and Data II Origination Q3 2010 76916.8 7.30 7300.00 291130.1 2.1E+09 2125.25 4.69 NA NA NA NA NA NA NA Q4 2010 86872.1 7.10 7100.00 328810.9 2.3E+09 2334.56 5.15 NA NA NA NA NA NA NA Q12011 73360.0 7.00 7000.00 277667.6 1.9E+09 1943.67 4.29 NA NA NA NA NA NA NA Q2 2011 80334.6 7.00 7000.00 304066.5 2.1E+09 2128.47 4.69 NA NA NA NA NA NA NA Q3 2011 97535.0 6.60 6600.00 369170.0 2.4E+09 2436.52 5.37 NA NA NA NA NA NA NA Q4 2011 109043.5 7.00 7000,00 412729.6 2.9E+09 2889.11 6.37 NA NA NA NA NA NA NA Q12012 101616.8 7.10 7100.00 384619.6 2.7E+09 2730.80 6.02 NA NA NA NA NA NA NA Q2 2012 87759.1 7.10 7100.00 332168.2 2.4E+09 2358.39 5.20 NA NA NA NA NA NA NA Q3 2012 80006.0 7.10 7100.00 302822.7 2.2E+09 2150.04 4.74 NA NA NA ' NA NA NA NA Q4 2012 71596.0 7,00 7000.00 270990.9 1.9E+09 1896.94 4.18 NA NA NA NA NA NA NA Q12013 58716.8 7.36 7360,00 222243.1 1.6E+09 1635.71 3.61 16677.4 58.0 58000.0 63124.0 3661189622.0 3661.2 8.07 Q2 2013 65603.4 6.30 6300.00 248308.9 1.6E+09 1564.35 3.45 25523.2 50.2 50200.0 96605.3 4849586662.4 4849.6 10.69 Q3 2013 63515.4 7,22 7220.00 240405.8 1.7E+09 1735.73 3.83 25592.9 29.7 29700.0 96869.1 2877013057.1 2877.0 6.34 Q42013 60233.6 7.84 7840.00 227984.2 1.8E+09 1787.40 3.94 24952.2 45.2 45200.0 94444.1 4268872280.4 4268.9 9.41 Totals Since Q3 2010 1113109.1 65.51 92745.7 34.52 Highlighted cells are the total for the current quarter Table 4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped TW4-24 TW4-25 i I Total Total ,, Total Total Pumped Cone Cone Pumped Total Total Pumped Cone Cone Pumped Total Total Quarter (gal) (mgll) (ugll) (liters) Total (ug) (grams) (pounds) (gal) (mgll) (ugll) (liters) Total (ug) (grams) (pounds) Calculations II I and Data I li Origination Q3 2010 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q4 2010 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q12011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q2 2011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q3 2011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q42011 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q12012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q2 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q3 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q4 2012 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Q12013 144842.6 35.9 35900.0 548229.2 19681429751.9 19681.4 43.39 99369.9 9.0 9000.0 376115.1 3385035643.5 3385.0 7.46 Q2 2013 187509.3 23.7 23700.0 709722.7 16820428001.9 16820.4 37.08 147310.4 5.2 5240.0 557569.9 2921666087.4 2921.7 6.44 Q3 2013 267703.5 32.6 32600.0 1013257.7 33032202568.5 33032.2 72.82 145840.9 5.69 5690.0 552007.8 3140924419.0 3140.9 6.92 Q42013 260555.3 34.6 34600.0 986201.8 34122582643.3 34122.6 75.23 126576.5 6.10 6100.0 479092.1 2922461520.3 2922.5 6.44 - Totals Since Q3 2010 860610.7 228.52 519097.7 27.27 Highlighted cells are the total for the current quarter Table4 Quarterly Calculation of Nitrate Removed and Total Volume of Water Pumped lWN-02 Total Removed Total Total by All Pumped Cone Cone Pumped Total Total Wells Quarter (gal) (m~) (~) (liters) Total (ug) (grams) Jpounds) (pounds) I Calculations and Data Origination Q3 2010 NA NA NA NA NA NA NA 15.69 Q4 2010 NA NA NA NA NA NA NA 27.97 Q12011 NA NA NA NA NA NA NA 73.30 Q2 2011 NA NA NA NA NA NA NA 27.01 Q32011 NA NA NA NA NA NA NA 16.82 Q4 2011 NA NA NA NA NA NA NA 19.71 Q12012 NA NA NA NA NA NA NA 15.86 Q2 2012 NA NA NA NA NA NA NA 15.D3 Q3 2012 NA NA NA NA NA NA NA 14.67 Q4 2012 NA NA NA NA NA NA NA 14.92 Q12013 31009.4 57.3 57300.0 117370.6 6725334176.7 6725.3 14.83 95.73 Q2 2013 49579.3 57.7 57700.0 187657.7 10827846433.9 10827.8 23.87 91.71 Q3 2013 50036.5 80.0 80000.0 189388.2 15151052200.0 15151.1 33.40 176.53 042013 49979.9 111.0 111000.0 189173.9 ___1Q9~305286.5 20998.3 46.29 162.07 -- Totals Since Q3 2010 180605.1 118.39 767.Dl Highlighted cells are the total for the current quarter Q2 Location 2010 MW-30 15.8 MW-31 22.5 MW-5 ND MW-11 ND ND =Not detected NS =Not Sampled Table 5 Nitrate Data Over Time for MW-30. MW-31. MW-5. and MW-11 ' ' . Q3 Q4 Q1 Q2 Q3 Q4 Q1 Q2 Q3 Q4 2010 2010 2011 2011 2011 2011 2012 2012 2012 2012 15 16 16 17 16 16 17 16 17 18.5 21 20 21 22 21 21 21 20 21 23.6 NS 0.2 NS 0.2 NS 0.2 NS 0.1 NS ND ND ND ND ND ND ND ND ND ND ND Q1 Q2 Q3 Q4 2013 2013 2013 2013 21.4 18.8 17.6 19.5 19.3 23.8 21.7 23.9 NS ND NS 0.279 ND ND ND ND ---- TABLE 6 Slug Test Results (Using KGS Solution and Automatically Logged Data) Well K (cm/s} MW-30 1.0E-04 MW-31 7.1 E-05 TW4-22 1.3E-04 TW4-24 1.6E-04 TW4-25 5.8E-05 TWN-2 1.5E-05 TWN-3 8.6E-06 Average 1 Average2 Average 3 Average 4 Notes: Average 1 = arithemetic average of all wells Average 2 =geometric average of all wells K (ft/day} 0.28 0.20 0.36 0.45 0.16 0.042 0.024 0.22 0.15 0.32 0.31 Average 3 = arithemetic average of MW-30, MW-31, TW4-22, and TW4-24 Average 4 =geometric average of MW-30, MW-31, TW4-22, and TW4-24 cm/s = centimeters per second ftlday = feet per day K = hydraulic conductivity KGS = KGS Unconfined Slug Test Solution in Aqtesolve TM. N:\WMM\Required Reports\Nitrate Quarterly Monitoring Report\2013 04\hydrogeochem\FiowCalcs: Table 6 TABLE 7 Pre-Pumping Saturated Thicknesses Depth to Depth to Water Saturated Thickness Well Brushy Basin Fourth Quarter, 2012 Above Brushy Basin (ft) (ft) (ft) TW4-22 112 53 58 TW4-24 110 55 55 Notes: ft =feet N:\WMM\Required Reports\Nitrate Quarterly Monitoring Report\2013 04\hydrogeochem\FiowCalcs: Table 7 TABLE 8 Pre-Pumping Hydraulic Gradients and Flow Calculations Pathline Boundaries Path Length Head Change Hydraulic Gradient (ft) (ft) (ft/ft) TW4-25 to MW-31 2060 48 0.023 TWN-2 to MW-30 2450 67 0.027 average 0.025 1 min flow (gpm) 1.31 2 max flow (gpm) 2.79 Notes: ft =feet ftlft = feet per foot gpm = gallons per minute 1 assumes width = 1,200 ft; saturated thickness = 56ft; K = 0.15 ft/day; and gradient= 0.025 ft/ft 2 assumes width = 1,200 ft; saturated thickness =56ft; K = 0.32 ft/day; and gradient= 0.025 ft/ft N:\WMM\Required Reports\Nitrate Quarterly Monitoring Report\2013 04\hydrogeochem\FiowCalcs: Table 8 INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and Field Data Worksheets Tab C Kriged Current Quarter Groundwater Contour Map, Capture Zone Map, Capture Zone Details Map, and Weekly, Monthly and Quarterly Depth to Water Data Tab D Kriged Previous Quarter Groundwater Contour Map Tab E Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells Tab F Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Tab G Laboratory Analytical Reports Tab H Quality Assurance and Data Validation Tables H-1 Field Data QNQC Evaluation H-2 Holding Time Evaluation H-3 Analytical Method Check H-4 Reporting Limit Evaluation H-5 QNQC Evaluation for Sample Duplicates H-6 QC Control Limits for Analyses and Blanks H-7 Receipt Temperature Evaluation H-8 Rinsate Evaluation Tab I Kriged Current Quarter Isoconcentration Maps Tab J Analyte Concentration Data Over Time Tab K Concentration Trend Graphs Tab L CSV Transmittal Letter Tab A Site Plan and Perched Well Locations White Mesa Site TW4-19 ffi MW-5 • TW4-12 0 TWN-7 0 PIEZ-1 perched chloroform or nitrate pumping well perched monitoring well temporary perched monitoring well temporary perched nitrate monitoring well ~ perched piezometer TW4-32 ~ temporary perched monitoring well installed September, 2013 RUIN SPRING b seep or spring HYDRO GEO CHEM,INC. APPROVED ,. IIIWlOI ~ ~ ~ lWNoOJ • 1ofW;tt 'f\1$~ ~· . 'f&o1 SITE PLAN SHOWING PERCHED WELL AND PIEZOMETER LOCATIONS WHITE MESA SITE DATE REFERENCE H:/718000/feb14/Uwelloc1213.srf FIGURE A-1 TabB Order of Sampling and Field Data Worksheets Name Nitrate Mg/L Previous Qrt. Nitrate Samples Date/Purge sample TWN-7 0.835 I IOj (bJI:\ I D~"Z.b TWN·l TWN-4 TWN-18 TWN-3 TWN·2 Duplicate of Rinsate DISamp/e 1.24 1.58 2.04 20.9 80.0 -rwJJ -.;I "'j".vr.J-!.J & J:~.J..v-'a Plez 1 7.83 P/ez2 0.198 Plez 3 1.81 · \1.)/\t,/i~ 01'2..1 iO/i/,//'3 oz l'i 101ll>!l3 og:s& 10117/13 Ot:.27 \C/ 16/1:.\ DCfSD \o { tt i•J 0 1 t. 7 lv h~h:J 012.4 iu/•7/1.3 og'-{5 \0/ li./\ '!I \1 0..5 ,o/lt.t n iDiO 10/il,/ I 3 I C.3-.1) u Nitrate Order 4th Quarter 2013 Depth Total Depth 112.5 125.7 145 96 96 ( Rinsate Samples Name Date Sample TWN-7R I TG 11'5/ IC TWN·1R TWN·4R TWN·lBR TWN·3R TWN·2R Samplers: Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I L)T1-I Qv.~der" 1\J iff'jp\fc.. '201~ Location (well name): '-I ....:.Pi..:.1=e.-c.=--~-=O:..:.I _________ ____J Sampler Name and initials: Field Sample ID Date and Time for Purging I \0/ l'/-z01'3 and Sampling (if different) Well Purging Equip Used: IQ]pump or ~bailer Well Pump (if other than Bennet) See instruction I N'/4 Purging Method Used: [QJ2 casings IQ]3 casings Sampling Event I Q\J:o-r+G('b .10~+.-.... f-t. Prev. Well Sampled in Sampling Event I p,· G'Z.-0.3 pH Buffer 7.0 /.0 pH Buffer 4.0 ~-" Specific Conductance!.._ _4_'1_~ ____ _,1~-tMHOS/ em Well Depth(O.Olft): ._I _o ____ __, Depth to Water Before Purging I f-2, r{D Casing Volume (V) 4" ~cll:~_o ___ ~,(.653h) 3' Well :_ " _ (.367h) Weather Cond. Ext' I Am b. Temp. ·c (prior sampling event)LI..;;;.6_0 __ _...J Time I \\Ot.j I Gal. Purged I () I Time I I Gal. Purged I I Conductance 1-z.lls I pH I g,73 I Conductance I I pHI I Temp. °C I t~.46 I Temp. oc I I Redox Potential Eh (mV) l:;rz.7 I Redox Potential Eh (m V) I I Turbidity (NTU) I 9.D I Turbidity (NTU) L J Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. °C I I Temp. °C I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I -0 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T=2V/Q= I tJ I 0 6 Name of Certified Analytical Laboratory if Other Than Energy Labs Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D D 3x40 ml D D HCL D D Nutrients ~ D lOOml D ~ H2S04 ~ D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologies D D 250 ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) ~ D Sample volume D ~ 0 ~ c'nlor:J( If preservative is used, specify Type and Quantity of Preservative: Final Depth I 6::). SD Sample Time \10_5 See instruction Comment Arr;v-ea on .s:tc o...f lOSO. -r..,,,er1 G---.rr:,. J D«n o..U prc.S-e11f -h co }7f!!.c-J-.St:4...,f1~. SC\Mpl~ h._,'leA "\t!J c=.ol)-eLi-cA c:o.:+ liO.S 'l.,)~+c:r \A)e..,S f\1.o,sf~ GJ~-r. LeJ:!-.S j-}<:. ~~ )\ 12.. Piez-01 10-16-2013 loo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I yn G.v:c;;fcr "'l+rJ't zotS Sampler Name See instruction Location (well name): '-1 _pj_.1o::~:..:"Z:....-...;O~~..::::.._ ________ __, and initials: I -r;..,ner Ho iJ;J~j M Field Sample ID Date and Time for Purging I lu/U./ 'ZOI~ and Sampling (if different) Well Purging Equip Used: IQ]pump or [][)bailer Well Pump (if other than Bennet) I N/A Purging Method Used: IQ]2 casings IQ]3 casings Sampling Event I Qu.G.r-\-u\"\ N ,±ro..ts Prev. Well Sampled in Sampling Event Ll_-r\_w_JJ_-_o_z _____ -' pH Buffer 7.0 /.0 pH Buffer 4.0 '-U5 Specific Conductance '-1 -'Cf-'<1-.:~ ____ _.l ~MHOS/ em Well Depth(O.Olft): ._I _o ____ ......... Depth to Water Before Purging I 3Z ,g~ Casing Volume (V) 4" Well:~_o ___ ---i,(.653h) 3" Well:_ o . (.367h) Weather Cond. Ext'l Amb. Temp. oc (prior sampling event)LI...:::b_11 __ ......~ Time I ll:>O'\ I Gal. Purged I 0 I Time I I Gal. Purged I I Conductance I 7Dl I pH I 7.Lt5 I Conductance I I pHI I Temp. oc ll>.47 I Temp. oc I I Redox Potential Eh (mV) I z qo I Redox Potential Eh (m V) I I Turbidity (NTU) I b.!> I Turbidity (NTU) I J Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I 'D Time to evacuate two casing, volumes (2V) T=2V/Q= I ~ I Number of casing volumes evacuated (if other than two) l o If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labsl L.. ...ce-£..:W~A:....l.. _____ ----J Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y VOCs D D 3x40 ml D 0 HCL D Nutrients ~ D 100 ml 0 ug H2S04 ~ Heavy Metals 0 D 250 ml D D HN03 0 All Other Non Radiologies D D 250ml D D No Preserv. 0 Gross Alpha 0 0 I,OOOml D D HN03 D Other (specify) ril D Sample volume D ~ D Ghlor;k, If preservative is used, specify Type and Quantity of Preservative: Final Depth '-'-1 ~~·-1 j..__ __ ___, Sample Time \010 Comment Arriv~a or'\ s•1-c ~ ~ 6.tl~ GoH~ ~flt:'$. L~ s.i+G {A.+ )Ol't See instruction --r', .. M,er 1 G-o-.t"ri11 1 Dee" ~n pn::s~.} -h. b.,.rJ CI>JI-uJ-cJ ~}'OlD. wo..ier w~ Mt::Ei.f~ G)ea.r~ Piez-02 10-16-2013 JDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D 0 D D D ~ 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I lf'h Qu.o.rl"er A:J;:tfl,J~ -z.of3 ~ See instruction Location (well name): ~.-l __;p_,_·-e_"Z..;...-_D_3 _________ _, Sampler Name and initials: 1..-r;. ... ,..cr No u:IJ ;J/'1t1 Field Sample ID Date and Time for Purging I \ D/J fo/ ZOI~ and Sampling (if different) .......,/A ~-~-------~ Well Purging Equip Used: [QJ pump or [ID bailer Well Pump (if other than Bennet) ..V/..4 ~~~-----~ Purging Method Used: @2 casings 1![]3 casings Sampling Event I o~c.r"tcrb 1\);+(~fc Prev. Well Sampled in Sampling Event ~.-I_P_i_-c:_-z_~_az.. ______ ~ pHBuffer7.0 ._1_1_,0 ___ _. pH Buffer 4.0 Lj.o Specific Conductance ._I -~'-'1'-'1 ____ _,h.tMHOS/ em Well Depth(O.Olft): ._I _0 ____ __, Depth to Water Before Purging I 1...\S, '\5 Casing Volume (V) 4" Well.:~_o ___ --1,(.653h) 3" Well:_ 0 . (.367h) Weather Cond. Ext'l Am b. Temp. oc (prior sampling event)'--1 ~6-"--~ Time I \03~ I Gal. Purged I !> I Time I I Gal. Purged I I Conductance I -z. ~ L-1-:::, I pH I ll, bn I Conductance I I pHI I Temp. oc I ~~.51 I Temp. oc I I Redox Potential Eh (mV) I '2..37 I Redox Potential Eh (m V) I I Turbidity (NTU) I ~.r: I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged ' gallon(s) Pumping Rate Calculation Flow Rate Q). in gpm. Time to evacuate two cas ing volumes (2V) s16o = ._I ...........;.o ___ ...J T=2V/Q= In I Number of casing volumes evacuated (if other than two) l o If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs I ...... A~\fJ-~_1--______ __, Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y VOCs 0 0 3x40 ml 0 0 HCL 0 Nutrients ~ 0 100 ml D ~ H2S04 ~ Heavy Metals 0 0 250 ml 0 0 HN03 D All Other Non Radiologies 0 0 250 ml 0 0 No Preserv. 0 Gross Alpha 0 0 I,OOOml 0 D HN03 0 Other (specify) 'tJ 0 Sample volume 0 !!! D Ghlor;~<. If preservative is used, specify Type and Quantity of Preservative: Final Depth ._I _5_7_._7_2 __ _. Sample Time ._l_10_3b ___ __. See instruction Comment Arri'lld on strc (;A.':t l025.~ner, C-o..rr:nl De-QJ I tJ./1 pr~C/1-r -h. .be...'] .!lf.i~~ ~~]e3 bc;,.;Jd a.-1-}03.5. \).)~er '...)4-S \'t'lDSi1..j Oe~.r. L.Jf S ;-h: ~t 1041/ Piez-03 10-16-2013 lno not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ~ 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2 -Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I 4Th Qu.~r+« .N i+r ... fc:. -z.o l3 See instruction Location (well name):!,_ _T_W-"W_-_0_1 _________ __, Sampler Name and initials: 11":nna Jt.lliJ'\j/--rH Field Sample ID Date and Time for Purging ._I ...;..lt>-'/--'~ ........ /_-z.;...o....:.\).....__~~~_.1 16/lbJ2oll' and Sampling (if different) ...v/A '-----------~ Well Purging Equip Used: 00 pump or [QJ bailer Well Pump (if other than Bennet) I 6-riAnJOf'o..S Purging Method Used: 002 casings @]3 casings Sampling Event I Q ~o..rf.srl!:J ;vif1'~=t<. Prev. Well Sampled in Sampling Event ._l_...,-_w_AJ_-_0_7 _____ ~ pH Buffer 7.0 L-1_7...:....;..;;.0 ___ ---l Specific Conductance ._I _'1.:...'1-'-j+-----~~ !!MHOS/ em Depth to Water Before Purging I .Sz;.c:to Weather Cond. Time I 0/~l.f I Gal. Purged I 55 Conductance I g~o I pH I "-'1~ Temp. °C 11'\.5'\ I Redox Potential Eh (m V) I :!"9 I Turbidity (NTU) I Zl:JO I Time I CY7Zf. I Gal. Purged I i7 Conductance I ~S'q I pH 1 7 .-zn Temp. °C 1'9·bl I Redox Potential Eh (m V) 1 3~5 I Turbidity (NTU) 15b I White Mesa Mill Field Data Worksheet for Groundwater I I I I pH Buffer 4.0 Y.o Well Depth(O.Olft): '-1 _11_'2._._5_0 __ __, Casing Volume (V) 4" Well:! 3b.3D 1(.653h) 3" Well:._. _o ___ ~. (.367h) Ext' I Am b. Temp. 0( {prior sampling eventl.._l .;;.e:,_• __ ...J Time I o1'2S I Gal. Purged I bb I Conductance I ~g1 I pH I (.,}'/ I Temp. oc I 1 ~.~1 I Redox Potential Eh (m V) 1591 I Turbidity (NTU) I 'Sb .-z. I Time 1017.7 I Gal. Purged I g~ I Conductance I B~ I pH 11. z.Z I Temp. oc I ]q, z;;g I Redox Potential Eh (m V) I 3'50 I Turbidity (NTU) I S~ I 1 of2 Mill -Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP} Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q) in gpm. Time to evacuate two casing volumes (2V) S/60 = I ll T = 2V /Q = I b. w I Number of casing volumes evacuated (if other than two) l o If well evacuated to dryness, number of gallons evacuated If) Name of Certified Analytical Laboratory if Other Than Energy Labs Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs 0 0 3x40 ml 0 0 HCL 0 0 Nutrients Bl 0 100 ml 0 [81 H2S04 ~ 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 Al'l Other Non Radiofogic,s 0 0 250ml 0 0 No Preserv. 0 0 Gross A lpha 0 D 1,000 ml D D HN03 0 0 Other (specify) ~ 0 Sample volume D r,l 0 ~ c.\, \ot")ae.. If preservative is used, specify Type and Quantity of Preservative: Final Depth I 17, '55 Sample Time 07Z/ See instruction Comment TWN-01 10-16-2013 IDa not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan {QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I q J ~ b>"'GV1=er /\H+r~1"t::-'2..013 See instruction Location (well name): ._l_:r..l......;W~N;:;.._-_o_-z.. ________ __J Sampler Name andinitials: I =r:,,u-tloJJ~d4.j /IB Field Sample ID Date and Time for Purging l l0/1"/'ZOI~ and Sampling (if different) L--....V.-~_~.:__ ______ __J Well Purging Equip Used: 00 pump or [QJ bailer Well Pump (if other than Bennet) I C"n:}Jt'l u.O~ Purging Method Used: [QJ2 casings [QJ3 casings Sampling Event I Q..,..().r-\-e .-h N rh·J; Prev. Well Sampled in Sampling Event .... 1_-ri_ltJ_W_-_0.3 ______ __, pH Buffer 7.0 pH Buffer 4.0 4.0 Specific Conductance ._I 9....:...:.~-Lj ____ _,I ~-tMHOS/ em wen Depth(O.Olft): L-1 _~_z;_.o_o __ ___, Depth to Water Before Purging j 'Z./. Z:"' Casing Volume (V) 4" Well:l L.Jl:\.{3 1(.653h) 3'' Well: o (.367h) L.......='------' Weather Cond. Ext'l Amb. Temp. oc (prior sampling event)L.,;I b=---6 __ _, Time I ~q q tJi I Gal. Purged I ~ 0 I Time I I Gal. Purged I I 0 Conductance 1357"1:, I pH I 6.C:3 I Conductance I I pHI I Temp. oc I \1>.5'1 I Temp. oc I I Redox Potential Eh (mV) I ~0 I Redox Potential Eh (m V) I I Turbidity (NTU) I l'} I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q) in gptl1. S/60= I Jg.6 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two ca ·ing volumes (2V) T= 2V/Q= I 0 I lo I ~ Name of Certified Analytical Laboratory if Other Than Energy Labs Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y VOCs D 0 3x40 ml D D HCL 0 Nutrients 'El D 100 ml 0 t9 H2S04 ~ Heavy Metals D D 250 ml D D HN03 D All Other Non Radiologies 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 D 1,000 ml 0 D HN03 0 Other (specify) "jJ 0 Sample volume 0 'ID 0 Ghlor;dc If preservative is used, specify Type and Quantity of Preservative: Final Depth 1 ...... _~_.,_· ___ _. Sample Time q3.Lll . See instruction Comment Ar .. ~\le.d on s.~te ri!'" D~L1 4. ~-.n-er 1 G_.,.J..,, Pe-Cfl G\11 pre::.ctd-+o coJlc:d-:seo""fl~s, S:,o.rr~p\c..s Goi\ed-ca tA.+ oqf.D. L~+\-.S ;-3z: o.f O'JSL.f, ~4--c:r l.Dc.t.S c.lc;o.r-, TWN-02 10-16-2013 lno not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D ~ 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I 91 h Q"'~r:h~r .AJ :+r.,d:c, Z013 Location (well name): IL-Ti_w_A>_~_C>3 __________ __. Field Sample ID Sampler N arne and initials: See instruction Date and Time for Purging ._P_o_)_IV_l._o_n _____ ___. and Sampling (if different) 10 )17/zot3 Well Purging Equip Used: (![]pump or jiD bailer Well Pump (if other than Bennet) G"rv.ndfd"os Purging Method Used: IT:[] 2 casings jiD 3 casings Sampling Event I Gv.~r:b::r 8 A) ~ol\f<. Prev. Well Sampled in Sampling Event l.____~_~_w_;v_-_18 _____ __, pH Buffer 7.0 pH Buffer 4.0 Specific Conductance 1~.-_0!_'f...,i ____ _JI ~-tMHOS/ em Well Depth(O.Olft): ~..1 _'i;_,_.o_o __ ___. Depth to Water Before Purging I '37. 2.D Casing Volume (V) 4" WeJJ:I :S&-~'1 ,(.653h) 3" Well: n (.367h) L---------1 Weather Cond. Ext'l Amb. Temp. oc (prior sampling eventll,_ 5_' __ __, Time I 0'9~ I Gal. Purged I 5'2. I Time I I Gal. Purged I I Conductance I ZL\";)g I pH I z;.~:c I Conductance I I pHI I Temp. oc I 'I'\ ."19 I Temp. oc I I Redox Potential Eh (m V) I :zgg I Redox Potential Eh (mV) I I Turbidity (NTU) 1 bl I Turbidity (NTU) I I Time I Ob1:7 I Gal. Purged I D I Time I o,,g I Gal. Purged l o I Conductance 124545 I pH I7.Z'L I Conductance I -z..ct=,~ I pH I 7·11 I Temp. OC 1 1~.so I Temp. oc I Jq .q7 I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 5Z gallon(s) Pumping Rate Calculation Flow Rate (Q)., in gpm. S/60 = 1..__--'\:..:L.J __ ___J Time to evacuate two casing volumes (2V) T=2V/Q= I ,_qg I Number of casing volumes evacuated (if other than two) 11.35 If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs L..l ~A.:..W---=-.:A:....L.. _____ ----.~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs 0 0 3x40 ml D 0 HCL 0 0 Nutrients [i 0 100 ml D l!l H2S04 ~ 0 Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologies 0 D 250 ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml D 0 HN03 D 0 Other (specify) ~ D Sample volume D 1St D ~ G ~)orid-c... If preservative is used, specify Type and Quantity of Preservative: Final Depth l._q_3_:z_o ___ __. Sample Time See instruction Comment Arr;-.JeA on s;+c:. ~ O'i Zl ~t1nCI' I &~ .. .,.;fl} t:>~~/1 ~11 pr~~'C(I-r ~( f'"'("~~~ Pv.r~ be"t.VJ ~1 043\. Pv.r~c~ l..)e\l for-,... 1-J-,._\ oJ:' Li rVJ;J1,,.,;te.5 ~ 45 .S~G£)nJs. R -eJ well J~ ~ VJ~t-(( w<A.S Mo~~ c.l<r.U. Pv.r~~ ~ntletl o..+ OCf:iS L-cJ:} s if~ ~t o~ Ardw:.J.. M\ ~,=f-t: q+ of... Z3, -r;,f'!et"" a.fiJ. G-""a;'l pr~sUJ-J-76 Gollc.c:,+ s~~.....,flo..i . D~p..J-h +o lll)o-..+c.r Wq5 3£ .77, _s,._,..,~J0 .b,.,,'Jc~ ad-0 f:.Z7, L& .$1:.}-c. a-J-0'3o TWN-03 10-16-2013 lno not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2 -frrata Gro~ndwater M_onitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA U~'IUM MILL : .(.~ See instruction FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I y~ Q ~ .-·\~,.. t\J -: \-r•\+-<':.--z.or~ Location (well name): ~.-1 :r--~--,;w:..:....:..:tJ:....-_0:::::..._:4 _________ ~ Sampler Name and initials: 1---r:t1t1<.r HG ii;J,~'l )-rl Field Sample ID I T WAl -0 _IDi6LOi:3 Date and Time for Purging I 1 0 I I (;,/-t-o i ·", and Sampling (if different) Well Purging Equip Used: @]pump or [gJ bailer Well Pump (if other than Bennet) Purging Method Used: 002 casings @]3 casings Sampling Event I '-"~Y+"C.rl "'\ .I\) ;tr~t-<: Prev. Well Sampled in Sampling Event L...l_-r_w_AJ_-_c_l _____ __J pH Buffer 7_0 /.0 pH Buffer 4_0 y .o Specific Conductance ~.-l _<i:....'1:....Jj~....._ __ __Jl ~MHOS/ em Well Depth(O.Olft): I rz.s :7o Depth to Water Before Purging I Y q. 02. Casing Volume (V) 4" Well:' s_o.o·7 ,(.653h) 3" WeiJ : D (.367h) '--"<------' Weather Cond. G\t:A.,r Ext'l Amb. Temp. "C (prior sampling event)~.-1 ..::2.:....." __ _J Time I O&ll I Gal. Purged I g,~ I Time I D& IZ. I Gal. Purged I Cf1:1 I Conductance I !OS9 I pH I /.11.--j I Conductance I IDf.O I pHI 7 .17 I Temp. °C I 1'4 .:\~ I Temp. oc I ~4 .4~ I Redox Potential Eh (mV) I -:wz. I Redox Potential Eh (mV) I 7;"1'1 I Turbidity (NTU) I 300 I ., ~ ] Turbidity (NTU) I '31D Time I ogt~ I Gal. Purged I ~10 I Time I O&l t I G-Jl. Purged I ~I I Conductance I IO.S6 I pH 17.1l( I Conductance 110 57 I pH I 7.18 I Temp. °C I }g .gg I Temp. oc [E.Y9 I Redox Potential Eh (mV) I -z..ttt,. I Redox Potential Eh (m V) I Z.'l'Z I Turbidity (NTU) I -~~{, I Turbidity (NTU) I )~S I White Mesa Mill Field Data Worksheet for Groundwater A 1 of2 capturx· COMPATIBLE WfTH,....-"-.... ..:Oii:r--fUHCTIONAUTY Mill -Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) . .. Volume of Water Purged [ Z.l gallon(s) Pumping Rate Calculation Flow Rate (Q) in gpm. S/60 = 1-j ____:1....~..\ ------1 Time to evacuate two c~sti1g volumes (2V) T = 2VIQ = I '1.1 () I Number of casing volumes evacuated (if other than two) I b If well evacuated to dryness, number of gallons evacuated Jo Name of Certified Analytical Laboratory if Other Than Energy Labs ._I ...~A:.!,.W.:.;..;..A'-=L;;:.._ ____ ____j Type of Sample VOCs Nutrients Heavy Metals Ail Other Non Radiologies Gross Alpha OtllCr (specify) C:h~or)Jc final Depth lt-..::t.:....o..:.:.5=-· ·.:....1 __ _...J ~ :1comment Sample Taken Sample Vol (indicate if other than as y N specified below) 0 0 3x40 ml ~ 0 IOOml 0 D 250m! 0 0 250 ml D D l,OOOml 1il D Sample volume Sample Time Filtered Preservative Type Preservative Added y N y N 0 0 HCL 0 0 D [:st H2S04 5(J' 0 0 D HN03 0 0 0 0 No Preserv. 0 0 0 0 HN03 0 0 D (jJ 0 0 If preservative is used, specify Type and Quantity ofPresetvative: See instmction A \ .l \ jr.:d ..-!" •. • L r> I I r d vetl. Of\ s.t--r~ 0.:1 0 .:;)~ . l '\nflt:r1 &-o..r r•11 , ~.z~n 4 1/ pre.S ~/'f'T 1--o ..-f·""r~e ,1nd '<~111ph,-,\j e veAJ-· fw-5~ b~j'u'l ;.f 0303 . 'Pu..r~e~ iAJe ll .Per •' +6ta.l ot II m;ov,-lc.__s. wr-1tcr Wtt.J •"-M.).k\) WJ,;f -e. bv.:t \.) ~ Slow~ c )c,;..r; :._J ·:Y'hn'-':.jh o ...::t-·1-\--.::.. pv..r~e. , 'P~r~c:. a.Je.~\ (lYl J. &.a Mple..$ U>/le<..~cl .,} oiS!Y . L,~{\--s ~h:. e.+ o JJ 11 . D-aT'\ ijo,1.,-jof\ w~·tl, 'the. s+cJ<. 0+ l}.t~h Qr\ ::.:+c. tc, spt+ SG.IVI:p}cs . ._ ________ -..~Do not touch this cell'(SheetName) White Mesa Mill Field Data Worksheet for Groundwater ~ 2 of2 Capturx· COMPATIBLE WITH_./'-W~<>rir--FUH<TIONALITY Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I Cfnl Gv."'rlcr 1\Hfrq.+e "Z.0)3 W See instruction Location (well name ):I~... _'"T'W __ tJ_-_0_1;........ ________ __, Sampler Name and initials: 1-=t";,~ No lh'J\:1/-r-fl Field Sample ID Date and Time for Purging I \0)15/zop and Sampling (if different) '--'-'lO=/'--'-'Ib/;;;..__Z_o--'13=-------' Well Purging Equip Used: [![)pump or [ill bailer Well Pump (if other than Bennet) I U'f "'~({Po5 Purging Method Used: 002 casings [QJ3 casings Sampling Event I Qu.&...-f-ertj A) i~c~"'h Prev. Well Sampled in Sampling Event I --rw.N-.. Y1R pH Buffer 7.0 pH Buffer 4.0 t.t.D Specific Conductance L.l _4-L~..:.q..:... ___ ...Jl !J.MHOS/ em Well Depth(O.Olft): I05.oo Depth to Water Before Purging I 8'-.'10 Casing Volume (V) 4" Well:~...;;..ll.;..;..~gJ~---1~(.653h) 3" Well:. o . (.367h) Weather Cond. C.lov.J~ Ext'l Amb. Temp. oc (prior sampling eventl~...l _5_6 _ __, Time loi44 I Gal. Purged llt:J I Time I I Gal. Purged I I Conductance I \L.b\ I pH I b •~S I Conductance I I pHI I Temp. oc I ,g ,3~ I Temp. oc I I Redox Potential Eh (m V) I 3'-t~ I Redox Potential Eh (mV) I I Turbidity (NTU) I wg I Turbidity (NTU) I I Time j06ZS I Gal. Purged I l> I Time jObZb I Gal. Purged 10 I Conductance l ll'l't I pH I ;,Jq I Conductance 1 l :Z:oo I pHI 7.Jz I Temp. °C lllf,-z..Gt I Temp. oc I \q.3t I Redox Potential Eh (mV) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in grm. S/60 = ._I _);;..:.) __ ___, Time to evacuate two casing volumes (2V) T=2V/Q= I 2-Pi I Number of casing volumes evacuated (if other than two) I \. bO If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D D 3x40 ml D D HCL D D Nutrients ~ D 100 ml D M H2S04 ~ D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologies D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) riJ D Sample volume D I» D I}} G ~ lorrd(' If preservative is used, specify Type and Quantity of Preservative: Final Depth I \I ::..~! Sample Time I D6?.5 See instruction Comment 1\rr;"d, on ~i-h::. o.+ ol3g' . ..,-;nr1Gr' o.nal 6-tA-ff';t'l Pr-e.se.n-}-J: r f>""'r,e. 'fv.~~"<~ b1!.~~ oJ- 0/~3 P4cJ w-e~~~ ~... 1 Mi1lv.,i--c... liS St:.cor1J.s . fU\If'~d W'(,ll J.r(j. lNo..+u-LOoO ~ 1.·~~ I,,,.~ '.....r'J"\ 61.,\~a .. J-'-"1'-P·-1. \~ ~~t~ ~ 0"1'\b ArrhlGA 01\ ~n-e a.+ 0b1.0, -r;.nner ~,A G-o..rr•'., r<'G.S,1:_(\+ +o Go lie<:,+ .S~'VY~fles~ S tAl\'\ rle~ b"'".'Jea ~rtJ. c:.ol \ec.tc:J a..+-06ZS. Le-J+ S•'+e. a:t 0 <3<:lS De.~ h \NrJ-u l..l~ 47.0l TWN-07 10-15-2013 jDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I o/~ Qv.w-f~,... A) ~frO\.fe s~tv~pl ··~ (.0\~ See instruction Location (well name); ._l--'-r\\)'--'--'=..;...·,v_-_0--'7_R....;..._ _______ __, Sampler Name and initials: 1:::rc..nner Holi.'Jo.;i!rH Field Sample ID Date and Time for Purging I \0/15/7.0 13 and Sampling (if different) .__.M~:Ii'a;..;.... _______ _J Well Purging Equip Used: (!]pump or [QJ bailer Well Pump (if other than Bennet) ._I _""'..:...I.;...;A;.._ _____ -J Purging Method Used: !m2 casings 1m3 casings Sampling Event I QV\o.rtu·J~ N ;OJOr.o..+<. Prev. Well Sampled in Sampling Event ._I_AJ_V_A _______ __, pH Buffer 7.0 1.0 Specific Conductance L-1 ....:'1....:9_..:.'1 ___ --lh.t.MHOS/ em Depth to Water Before Purging 1~...-...;o:._ __ ---J Weather Cond. Time 1 072.3 I Gal. Purged ll3D Conductance I -z...'2. I pH I G..03 Temp. oc 114.\7 I Redox Potential Eh (m V) I :nzt I Turbidity (NTU) I 0 I Time I I Gal. Purged I Conductance I I pH I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater I I I I pH Buffer 4.0 4.0 Well Depth(O.Olft): ._I _o ____ _J Casing Volume (V) 4" WeJI:~~----11(.653h) 3" W II:_ 0 . (.367h) Ext'l Amb. Temp. ·c (prior sampling event)L-1 .5_0 __ _, Time I I Gal. Purged I I Conductance I I pHI I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) I J Time I I Gal. Purged I I Conductance I I pHI I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) I I 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged lSD gallon(s) Pumping Rate Calculation Flow Rate Q) in b'Pm. S/60 = ._I _l....J...l __ _.. Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two a ing volumes (2V) T=2V/Q= I 0 I lo lo Name of Certified Analytical Laboratory if Other Than Energy Labs ~..l_lt;....'W___;_A_L ______ ....~ Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D D 3x40 ml D D HCL D D Nutrients rn D 100 ml D I] H2S04 ~ D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologies D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) ~ D Sample volume D r!l D lSI c h \cH·;J-c If preservative is used, specify Type and Quantity of Preservative: Final Depth ._I -~0 ____ __, Sample Time 072.'-J See instruction Comment Arri\)e~ Ofl ~1i-c. o.,}07Jb -(..,.•ntef"" o.nJ &o..<r;" f~'eSeY'I.f -hr-r ,'n.so.+e . 'R t~.s~te be~"'n ~t 0710 'P V..f¥'1 r~~ 50 (}-~~. 11 0 ".J o.r ~o~p ~w+-c.r o.nt.\ JbO ~A110fi.S o.f' P:L w~-ler. ~tkfVl~\~ c. o I ~eG-\-e:~ tkl 677..Y L~ -R-.s 1i-e.. ~J 0'77.7 TWN-07R 10-15-2013 Jno not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I Yf\\ GJ\AO..<"'ler 1\)fTrt.:«c... "2:0 1'3 Location (well name): .__1_"'11_· _W...:...AJ..;...-_l:..:::g'--------------J Field Sample ID Sampler Name and initials: See instruction -· Date and Time for Purging I 10/l 'Jzo.c and Sampling (if different) L---"'-/-~-------___J Well Purging Equip Used: ~pump or [QJ bailer Well Pump (if other than Bennet) &ri.Nf\Uo~ Purging Method Used: (ID2 casings [QJ3 casings I lw~'~'-O"l Sampling Event I Gv.~r:ft-rl,~ AJ ,·:},~:fo:: Prev. Well Sampled in Sampling Event._ _________ __, pH Buffer 7.0 7.0 pH Buffer 4.0 I t:J .o Specific Conductance ._I _'t_'\_'i ____ ..JI !!MHOS/ em Well Depth(O.Olft): 195.00 Depth to Water Before Purging I 58 ,i'f 4" Well:! ~b:2..~ ,(.653h) 3" Well: D (.367h) .___ ___ __, Casing Volume (V) Weather Cond. Ext'l Am b. Temp. ·c (prior sampling eventli'-'3""-• __ ____...J Time I 081;.5 I Gal. Purged I ,1 I Time I 08-S' I Gal. Purged I llO I Conductance 1 -z-zoo I pH I'· <6.5 I Conductance l zze~o I pHI ~-"E/ I Temp. °C lk' lG:~s 1 Temp. oc 1 rq.3ro I Redox Potential Eh (m V) I -z.211~ I Redox Potential Eh (m V) I Z. 11 I Turbidity (NTU) I H5r.5 I Turbidity (NTU) 1 l<>3"1 I Time I oa57 I Gal. Purged I n., I Time I oar;g I Gal. Purged I t3'f. I Conductance I 'Z:OZ:H5 I pH IE>·&S I Conductance I ·z:z.a t I pHI ~-!'5 I Temp. °C I lq.~t; I Temp. °C 119-'to I Redox Potential Eh (mV) I 2:~~ I Redox Potential Eh (m V) I 'Z<:flf I Turbidity (NTU) I JO~g I Turbidity (NTU) I Jostf I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q). in gpm. S/60 = I \\ Time to evacuate two ca ing volumes (2V) T = 2V/Q = I )0 .?..3 I Number of casing volumes evacuated (if other than two) l o If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs I._»_W_~_L _____ __, Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D 0 3x40 ml D 0 HCL 0 0 Nutrients 1!] 0 100 ml 0 ~ H2S04 -~ 0 Heavy Metals 0 0 250ml D D HN03 0 0 All Other Non Radiologies D 0 250ml D D No Preserv. 0 0 Gross Alpha D 0 1,000 ml 0 0 HN03 0 0 Other (specify) 'tl D Sample volume 0 ~ D lJ Ghlorla-c If preservative is used, specify Type and Quantity of Preservative: Final Depth I bO,'Z~ Sample Time ._I _tJ_S£>...:....::...8'_-----~ See instruction Comment A.-r:\Jdv Of\ ~rh:. 01.-t og~3 -rOI/IriC'j Cr~>-rritll D~I'}J .,_1} p~~~ ~r'" py,r~-e.~nJ .s~_,.,p1·~ ~l)ey;;/, Pv.r~.::_ be.jCV'> ~i-' ogLU -"'-J~d Vf51ls .f;.r (}.. +oi-to.\ b.f )"Z. V'llf\.v.+C4 ucd-cr IIJA...S. ... ,.,IJJ<~ aJJ,,ft: "b,J-'-"'6 ~low\~ ck ... ri'~ ~ro~ho\Nt 11--c.. fw-~~~ fu.r~c. ~,JeJ N"l~ 5~""p1c.S col7ec1-cJ q_..q-~J~ l& ~; r-r: ""+-0, 0"2. TWN-18 10-16-2013 loo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER DescriptionofSamplingEvent: I 11'1""-&\U\.rtef" C.nloro~rM ~01:3 [ See instruction Location (well name): I -=Fw>'j 'Zoe -rw l.\-2."2. Sampler Name and initials: I -r#-nth::r ffo IJ i(A,_., /111 Field Sample ID Date and Time for Purging I I0/2.'! /~O'(j and Sampling (if different) ~--,;..M...;0~14.;....._ _______ _, Well Purging Equip Used: [!!]pump or ~bailer Well Pump (if other than Bennet) I Go.o1+/f.l li\Ov\.S Purging Method Used: ~2 casings [QJ3 casings Sampling Event I &~-h:r b C"'\ot"'6.fb'rl""l Prev. Well Sampled in Sampling Event ~..l-rw __ Y_-_2._'-/ _____ ____. pH Buffer 7.0 7.0 pH Buffer 4.0 '-l.O Specific Conductance lo........;.~....;..~ ~f ____ _.1~-tMHOS/ em Well Depth(O.Olft): r.1 -i:I&f;ll)~,iiHoo~-~~ \ 13.5'D Depth to Water Before Purging I §it"O \ • b?.,bg Casing Volume (V) 4'1 Well:l ~1 .'!;0 .... ,(.653h) 3>~.1~ 3" Well:_ () _ (.367h) Weather Cond. Ext'l Amb. Temp. oc (prior sampling event) I-I ~13_8 __ ...... Time I \'Z. '2.' I Gal. Purged I 6 I Time I I Gal. Purged I I Conductance I 6383 I pH I 6 493 I Conductance I I pHI I Temp. oc I 15. LU I Temp. oc I I Redox Potential Eh (m V) I 2YZ I Redox Potential Eh (m V) I I Turbidity (NTU) I Q I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q) in gpm . S/60= I ~ \~.0 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two casing volumes (2V) T = 2V/Q = I l> I Name of Certified Analytical Laboratory if Other Than Energy Labs Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type VOCs Nutrients Heavy Metals All Other Non Radiologies Gross Alpha Other (specify) Cn 1or ,'Jc. Final Depth ._I _._17.;....'..;..:11'-------' Comment 01'\ 5-~h. ~~J c.olle.d-.:: a y N specified below) y N y Gl D 3x40 ml D ~ HCL f)il $ D 100 ml D In H2S04 129 D D 250 rnl D D HN03 D D D 250ml D D No Preserv. D D D 1,000 ml D D HN03 D 00 D Sample volume D ~ D If preservative is used, specify Type and Quantity of Preservative: Sample Time \'ZZ/ See instruction 1'2..2.'31. ~fll'\cr 6Jla GM,.;n pas.cn~ -h Gol!ec+-Sa.Mple.s. ~+ 12'2.1, W"'tcr v.:x:c.~ Gko.,r-, t.~} ~itc ":t )2.Z~ TW4-22 10-29-2013 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D ~ 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I ~ Q-A .,_<"fc.r GYI lorotorM 201,3 See instruction Location (well name): ~...1 _-r_w_L.J:....-_Z....:'i~---------1 Sampler Name and initials: 1--r;.fll'le.f Ho II ;J~~ )1f.} Field Sample ID Date and Time for Purging I IO/-z.~/2oiJ and Sampling (if different) NI'A '----~-------~ Well Purging Equip Used: (J[]pump or [QJ bailer Well Pump (if other than Bennet) I cOT\+;,IAOu..J Purging Method Used: @]2 casings [QJ3 casings I II.JL\-2-S Sampling Event IQv.().ffc:r 6 Gh I orotc!l r M Prev. Well Sampled in Sampling Event '---------------' pH Buffer 7.0 7.0 pH Buffer 4.0 4,1:> Specific Conductance ~...1_1--'-~-'i ___ ____.l~-tMHOS/ em Well Depth(O.Olft): 11?...5 0 Depth to Water Before Purging I b~. 2 0 Casing Volume (V) 4" Well:' '30, '2.3 ,(.653h) 3" Well: i5 (.367h) '-------l Weather Cond. I Ove.rca..si Ext' I Am b. Temp. oc (prior sampling event).__j1_3_0 __ _. Time ll2 \&j I Gal. Purged I 0 I Time I I Gal. Purged I I Conductance I ~o-z.q I pH I ~.8s I Conductance I I pHj I Temp. °C I 15.11 I Temp. oc I I Redox Potential Eh (m V) I -z'!;O I Redox Potential Eh (mV) I I Turbidity (NTU) I 0 I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. °C I I Temp. oc I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = I 1 ~.l'> Time to evacuate two n ing volumes (2V) T= 2V/Q =I 6 I Number of casing volumes evacuated (if other than two) 0 If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs ~.-I ...:A-=-W~A~L:::;._ ____ _.. Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y VOCs ijl D 3x40 ml D t¥1 HCL Ill Nutrients Ill D 100 ml D Ill H2S04 m Heavy Metals D D 250 ml D D HN03 D All Other Non Radiologies D D 250m! D D No Preserv. D Gross Alpha D D 1,000 ml D D HN03 D Other (specify) Ill D Sample volume D I[) D Cn\or~Jc. If preservative is used, specify Type and Quantity of Preservative: Final Depth I 731 2'1 Sample Time See instruction Comment .llrril.lec\ 01"1 ~ ;}c "'+ J"Z IS 1 ~hfl-er"' o.ntl. cTa.rr1'1\ f~t1+ +., coil-ed-" s.t,..,pl-e.s . 5.di.mple~ toll-ec.+~~ o;,j--12"2.0. wo...ter ~ ~ Gko..f". L ~ft .s ;.fc G\ -t )2'2.'- TW4-24 10-29-2013 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N D D D D D 12!1 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL See instruction FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I l.jTh Q "'t~.rf~,.. C.\-, 1 oro.f"on-¥1 2.013 Sampler Name Location (well name): I :fw4-'2..5 and initials: l-r;!)l1t:Y" Hl) n;Jq'1/m Field Sample ID Date and Time for Purging L-l __ \_0..;.../_1.--'"\"-/_:.2_0_.0=-----' and Sampling (if different) I N'(A Well Purging Equip Used: [g]pump or [QJ bailer Well Pump (if other than Bennet) Purging Method Used: [QJ2 casings [QJ3 casings Sampling Event l Qv.c>-l+c:.r\~ C.n I OnrtonVJ Prev. Well Sampled in Sampling Event L....I _M_W_-_3_::2. _____ __, pH Buffer 7.0 7.D pH Buffer 4.0 Y.O Specific Conductance ll.....-'9:.__~:.....4:....._ __ _,~1 ~MHOS/ em Well Depth(O.Olft): I \2,'-\. go Depth to Water Before Purging I 5 Z. D {) Casing Volume (V) 4" Weii :I SO.l5 1(.653h) 3'' Well : o (.367h) L-------' Weather Cond. Ext'l Amb. Temp. ·c {prior sampling eventlL-1 -'-)3_0 __ _.. Time 1 12.63 I Gal. Purged 10 I Time I I Gal. Purged I I Conductance I "2 I :S.C{ I pH l 7.oq I Conductance I I pHI I Temp. °C I n;; .ss I Temp. oc I I Redox Potential Eh (m V) I -z..r;;~ I Redox Potential Eh (m V) I I Turbidity (NTU) IZ5 I Turbidity (NTU) I J Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. °C I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flow Rate (Q) in gpm. S/60 = I 18'. 0 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Time to evacuate two ca in-g volumes (2V) T=2V/Q= I 0 I l o Name of Certified Analytical Laboratory if Other Than Energy Labs ._I ""'A;..;:\rJ_.A'-'-L ______ __. Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs !!I D 3x40 ml D BJ HCL ~ D Nutrients !1J D 100m] D ijl H2S04 rn D Heavy Metals D D 250m! D D HN03 D D All Other Non Radiologies D D 250m] D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) l'Sl 0 Sample volume 0 lSI D ~ Lh\o.-;Je If preservative is used, specify Type and Quantity of Preservative: Final Depth l 7C:. 4] Sample Time See instruction Comment Arri>Je.J.. c11 .s:+~ ,.t-11.5'1. -r;..l'lt'IV"' .-t,.,J 6-"'rr,',.. pre's en J-+.. co/J~c.1-.SqJ11;oleJ . .S~plc:.~ co/lech:J 01.~ }2.0 'i. INtA.+c:r \,.)c...s G \-e,o.r Le.f-1-s it e. "'J , z 07 Cof\~;nuo~ ?vM?;~ Well TW4-25 10-29-2013 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: YTh Giv..o.f4ei" c..\'llo-rbfortvl ZOI3 Location (well name): l._ii....;..._w_4_-_,_o __________ ___j Field Sample ID IIW4-b()_II I9 ZOJ'3 Sampler Name and initials: See instruction Date and Time for Purging 1-1 _n.;.;,./...:.t4_;,./_z_o_J:3 _____ __, and Sampling (if different) tJ/A ~~....;..._-------~ Well Purging Equip Used: Cf[]pump or [QJ bailer Well Pump (if other than Bennet) I 6-'(~"a+os Purging Method Used: (![]2 casings (g]3 casings Sampling Event I Q\AA(fcrb C.'nl or(;:::h>fiY'\ Prev. Well Sampled in Sampling Event I.___"T'_W_l.\_-_3_'1 _____ .....~ pH Buffer 7.0 7.0 Specific Conductance!._ _'1~~..;.."1 ____ _,1~-tMHOS/ em Depth to Water Before Purging l.__o ___ _, Weather Cond. Time I llG!;~ I Gal. Purged I D Conductance I o.s I pH I 6.41 Temp. °C I llf .o3 I Redox Potential Eh (mV) I '3qs I Turbidity (NTU) I \.~ I Time I I Gal. Purged I Conductance l I pH I Temp. °C I I Redox Potential Eh (m V) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater I I I I pH Buffer 4.0 4.6 Well Depth(O.Olft): ._l __ o ___ ___J Casing Volume (V) 4" Well :~_c __ -1,(.653h) 3" Well:_ 0 _(.367h) Ext'l Amb. Temp. oc (prior sampling event)._l ""-IS_' __ _, Time I I Gal. Purged I I Conductance I I pHI I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) I -' Time I I Gal. Purged I I Conductance I I pHI I Temp. oc I I Redox Potential Eh (m V) I I Turbidity (NTU) I I 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2 -Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 0 gallon(s) Pumping Rate Calculation Flow Rate JQ) in gp m. S/60 = I 0 Time to evacuate two casing volumes (2V) T=2V/Q= I 0 I Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated 0 Name of Certified Analytical Laboratory if Other Than Energy Labs ._I ..:.A..:..\,J.:...;,.tfr..~.,l...=---------J Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs Ci§ D 3x40 ml D [] HCL I2J D Nutrients ~ D 100 ml D 129 H2S04 rn D Heavy Metals D D 250m! D D HN03 D D All Other Non Radiologies D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) l3J 0 Sample volume D ~ 0 I:E Ghlor~~e If preservative is used, specify Type and Quantity of Preservative: Final Depth~~ _......;0::;.__ __ _. Sample Time 070b See instruction Comment TW4-60 11-14-2013 lno not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 WHITE MESA URANIUM MILL FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: I Y-rh Q"'l,\;1y..r N ;h .... =tc. zot3 , See instruction Location (well name): .... 1-n_w_N--=---....::b::....b _________ __. Sampler N arne and initials: ff; ... ncr-J.t ol J:J'\j/"f7'J- Field Sample ID Date and Time for Purging I 10/li/ZOI-3 and Sampling (if different) Well Purging Equip Used: ffi]pump or [QJ bailer Well Pump (if other than Bennet) Purging Method Used: [QJ2 casings [QJ3 casings r-=------r--.--...-T--....... ~-----1 'A-c:'Z. .... o 1 Sampling Event IQv.D;(f¢6 /\),:+;::~;(: Prev. Well Sampled in Sampling Event,_ _________ __. pH Buffer 7.0 7,0 pH Buffer 4.0 Specific Conductance ._I _q'-'i--'11------'1 ~-tMHOS/ em Well Depth(O.Olft): ._I _0 ____ __, Depth to Water Before Purging l.__o ___ __. Casing Volume (V) 4" Well:~-::i'J~---il(.653h) 3" Well:. 7) . (.367h) Weather Cond. Ext'l Amb. Temp. oc (prior sampling eventJ'-'Il'-E._0 __ _, Time I D~Y lf I Gal. Purged I 0 I Time I I Gal. Purged I I Conductance I Lc, I pH I ~...3b I Conductance I I pH I I Temp. oc I lb.Y~ I Temp. oc I I Redox Potential Eh (m V) I Z~'! I Redox Potential Eh (m V) I I Turbidity (NTU) I t5 I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (mV) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate lQ}, in gpm. S/60 = I 0 Time to evacuate two ·a ·ing volumes (2V) T = 2V/Q =I 0 I Number of casing volumes evacuated (if other than two) 1-o If well evacuated to dryness, number of gallons evacuated 0 Name of Certified Analytical Laboratory if Other Than Energy Labs '-1 J...A.:..\N;.....L.fo...;L;;;..._ ____ ___, Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D D 3x40 ml D D HCL D D Nutrients llJ D 100 ml D ~ H2S04 2!1 D Heavy Metals D D 250 ml D D HN03 D D All Other Non Radiologies D D 250 mJ D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) ill D Sample volume D l9 D ]ll Gh lorl~( If preservative is used, specify Type and Quantity of Preservative: Final Depth ._I ----'0~---....1 Sample Time 08l-1.5 See instruction Comment TWN-60 10-17-2013 IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1-2 ~..,..,,..,..,1Ls WHITE MESA URANIUM MILL See instruction FIELD DATA WORKSHEET FOR GROUNDWATER Description of Sampling Event: 11..\Th Qv.A.rrfc:r N ;fr.,.,foc. '2.6 D Location (well name): ~....I_""T'"W __ /\J_-_&5 _________ ___, Sampler Name and initials: I =t".,.,-(11'1 t1 flo 1 J.'d\,..j/--1'» Field Sample ID Date and Time for Purging I l0/1,/2..013 and Sampling (if different) ~.-..:..,..;....;../"'::....:~....:......---------' Well Purging Equip Used: [f[]pump or [Q] bailer Well Pump (if other than Bennet) I &< ~J"o ~ Purging Method Used: (1!]2 casings IQ]3 casings I -t"w/'J-07 Sampling Event I Qv..l'..r h .. r~ /\5 ;h;;a:"< Prev. Well Sampled in Sampling Event L-------------l pH Buffer 7.0 1.0 pH Buffer 4.0 I q,o Specific Conductance ~.-1 _q....:..q____:~ ___ _..l ~-tMHOS/ em Well Depth(O.Olft): Depth to Water Before Purging I S.C.. Gf 0 Casing Volume (V) 4" Well:l ~C.. 321 I (.653h) 3" Well:_ 0 (.367h) ..___ ___ __, Weather Cond. Ext' IAmb. Temp. oc (prior sampling event)L.l ....::,_0 __ _j Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp. oc I I Temp. oc I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I J Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHf I Temp. oc I I Temp. oc I I Redox Potential Eh (mV) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 06-06-12 Rev. 7.2-Errata Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged gallon(s) Pumping Rate Calculation Flow Rate (Q), in b'J)m. S/60 = 1..__1_\ __ ____. Time to evacuate two ca ing volumes (2V) T=2V/Q=I "·'() I Number of casing volumes evacuated (if other than two) 0 If well evacuated to dryness, number of gallons evacuated 0 Name of Certified Analytical Laboratory if Other Than Energy Labs A'WAL Sample Taken Sample Vol (indicate Filtered Preservative Added Type of Sample if other than as Preservative Type y N specified below) y N y N VOCs D D 3x40 ml 0 D HCL D D Nutrients ~ D IOOml 0 ~ H2S04 ~ D Heavy Metals D D 250 ml 0 D HN03 D D All Other Non Radiologies D D 250 ml 0 D No Preserv. D D Gross Alpha 0 D 1,000 ml 0 D HN03 D D Other (specify) cg 0 Sample volume 0 ~ 0 ~ 0 hj Of';J~ If preservative is used, specify Type and Quantity of Preservative: Final Depth I 71. '3S Sample Time 07Z7 See instruction Comment TWN-65 10-16-2013 IDa not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 TabC Kriged Current Quarter Groundwater Contour Map, Capture Zone Map, Capture Zone Details Map, and Weekly, Monthly and Quarterly Depth to Water Data TIME WELL 1211 MW-1 951 MW-2 1304 MW-3 1303 MW-3A 935 MW-5 939 MW-11 933 MW-12 917 MW-14 917 MW-15 1308 MW-17 1209 MW-18 1152 MW-19 1226 MW-20 1153 MW-22 931 MW-23 1233 MW-24 942 MW-25 1240 MW-26 1230 MW-27 1236 MW-28 948 MW-29 944 MW-30 821 MW-31 819 MW-32 923 MW-33 920 MW-34 929 MW-35 927 MW-36 918 MW-37 Static level 64.60 109.52 87.49 85.93 106.02 86.51 108.11 103.25 105.90 72.95 71.11 58.38 89.10 67.70 120.72 114.15 73.14 66.18 53.21 76.22 101.11 74.83 67.24 73.91 DRY 107.56 111.88 110.10 114.22 NAME: Garrin Palmer, Tanner Holliday, David Turk DATE: 12/20/2013 TIME 1238 802 806 809 1226 812 801 805 808 811 813 815 731 735 737 1240 817 819 1225 1242 1229 1223 1224 759 1242 1221 757 739 732 742 746 748 734 749 743 WELL MW-4 TW4-1 TW4-2 TW4-3 TW4-4 TW4-5 TW4-6 TW4-7 TW4-8 TW4-9 TW4-10 TW4-11 TW4-12 TW4-13 TW4-14 TW4-15 TW4-16 TW4-17 TW4-18 TW4-19 TW4-20 TW4-21 TW4-22 TW4-23 TW4-24 TW4-25 TW4-26 TW4-27 TW4-28 TW4-29 TW4-30 TW4-31 TW4-32 TW4-33 TW4-34 Static Level 69.10 64.66 65.45 51.85 70.16 60.18 68.93 65.27 64.84 57.86 58.02 57.99 42.11 46.48 84.58 66.18 61.85 73 .91 61.57 66.84 70.09 61.90 59.07 64.41 60.98 83 .91 62.71 80.80 36.75 71.61 77.00 82.77 48.10 70.11 69.20 TIME 1156 1150 1146 755 752 1227 1134 1139 1144 NA 1205 1214 NA NA NA NA NA NA 1157 NA 1201 NA 1141 1012 WELL PIEZ-1 PIEZ-2 PIEZ-3 PIEZ-4 PIEZ-5 TWN-1 TWN-2 TWN-3 TWN-4 TWN-5 TWN-6 TWN-7 TWN-8 TWN-9 TWN-10 TWN-11 TWN-12 TWN-13 TWN-14 TWN-15 TWN-16 TWN-17 TWN-18 TWN-19 Static Level 63.16 33.51 44.93 50.35 47.68 57.75 32.01 36.90 49.95 Abandon 76.79 87.03 Abandon Abandon Abandon Abandon Abandon Abandon 62.31 Abandon 47.71 Abandon 59.19 52.90 Some time may be the same because we split up to take measurments. TIME WELL Static Level NA DR-1 Abandon NA DR-2 Abandon 1246 DR-S 83.05 1248 DR-6 94.35 925 DR-7 91.86 1240 DR-8 51.11 1237 DR-9 86.47 1234 DR-10 78.15 1256 DR-11 98.25 1258 DR-12 89.90 1301 DR-13 69.79 1221 DR-14 76.33 1230 DR-15 92.91 NA DR-16 Abandon 1217 DR-17 64.97 NA DR-18 Abandon 1212 DR-19 63.00 1214 DR-20 55.50 1157 DR-21 101.29 1209 DR-22 DRY 1200 DR-23 70.62 1206 DR-24 43.80 NA DR-25 Abandon I Weekly Inspection Form Date ,of-, /-z.ct3 Name ~,-,(\e.r ~oii :J~{ 1 &c..rr;,., Pc.IMcr System Operational (If no note Ti .... !!!! WIJ e D h* e_pt c omments bl I • ' an!l ero ems corrective aottons} !'-101 MW-4 G,K80 Flow ~3 eYes )No Meter z:o7f3LJ,Z.S ~No ~ r3:>5& MW-26 bz .L\.5 Flow 100 ( Ye~No ~ Meter 3k.'1 lt71. o-z.., (Yes~o )~'SO TW4-19 b~·g4 Flow ~ Y. o QesJ No Meter 16.0\2 so.oc; ~No f-. t'3S3 TW4-20 g ,_qo Flow ~ '{8' (Yes )'.Jo Meter S cr3o~l.\ .'--17 '-.Ye§)No -1'-\D~ TW4-4 16 l\ Flow g.o (Yes\ No Meter let z. I IS~ .7 / ( Ye~ No - 1'3~'3 TWN-2 bO.O\ Flow jg.S (_~yJo Meter r::,'1'i 1~. b (Yes>o 1350 TW4-22 !;g.DD Flow .\~:z.. (Ye§\ No Meter bq fa 9 2.1 ~ ~Y~No ~ "' \]~7 TW4-24 75.C..I Flow I~.'?.. (-~0 Meter <"=.lt1~Dg.L., ( Ye.s) No l J. '10 TW4-25 64,5D Flow 18~ (Yes }Jo Meter '4o'Z.rl6 ~ (Yes)No - Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): --------------- * Depth is measured to the nearest 0.01 feet. Weekly Inspection Form ( Date Name 06("r.' ..... PD..\c:"'e,r. (c td'zec System Operational (If no note Tl me Wll e 0 h* ept c omments anv oroblems/corrective actions} I z. "4 l{ MW-4 G7. 71 Flow ~-4 6-1' -"'1 (Yes)-No Meter 2tZ7'Z.~ .g~ ~s'> No IZ'-10 MW-26 64.'l7 Flow I o. '-{ &PA ~ No Met.er 3Uo6¥ z. 7 (Vel· No - ll4l TW4-19 6().7'1 Flow 1'-t.o &~.M.. @ No Meter 1632"475.65 <Ye~ No l't.37 TW4-20 /J'1..13 Flow £1. 6 6-P..v\ {YeS\ No Meter .5Ci~ s :1."1. ~C> (Yes)No IZt.H TW4-4 6'7.(0 Flow 7.'-\ &P.M. -?Ye~ No Meter 1'16bOZ:.~k (YeS) No ......____ 12..25 -'---= . TWN-2 2/,'30 Flow IS .b GPJ>A-~No Meter ~~~ -z,t,.g, -ro (Ye?f No 12.33_ TW4-22 58.05 Flow \i( o trP..M-eYe~ No Meter 11~04 (Z (Yes".>io 1230 TW4-24 bb. 3ct Flow \K.o 6 f_,4A-~No Meter I, 3 8 2 q 7 -\0 ~s""j No IZ.ZO TW4-25 155.60 Flow IB.L\ GP.fA... eYe$) No Meter 4 118'78'. 70 ~No ---- Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): ---------------- * Depth is measured to the nearest 0.01 feet. ( Weekly Inspection Form Date 10 1 z.3 k~ System Operational (If no note r· 1me wn e D h* e__gt c omments an31: QYO bl I ctfv ' ) ems corre e actions I 4 46 MW-4 sg.zo Flow y .J &P..,.v\. ~No Meter 21C\16t.'Z7 (!_ej} No l_l:f.3_£j MW-26 87.16 Flow JO. o 6-P.-v\. d"e]) No Meter 368...C78,67 ~'\ No I 5o~ TW4-19 6o. zb Flow I 4.0 6-P.M (Yes_) No Meter r67Z777.~o C(e§) No 1'135 TW4-20 65.3o Flow ID. \ GP.I-A. ~S)No Meter 5q6 t.( ID. Z3 (Y~ No I 1.-{,.SO TW4-4 18. 7f Flow 7-Z. 6-PrA-{Yej No Meter Z.DZ6«Z. go (Ye§) No 14 21.{ TWN-2 Z$;.6Z.. Flow ]$; I &(JM (Y~ No Meter 1'-\jO~'f 60 ((e~ No I y32. TW4-22 .5'ct .3Cj Flow /f. z.. GPA ?(~No Meter ll.(oso. 6o (Ye§} No I I.J'ZJ! TW4-24 66-6"0 Flow I g,o GPM. ~No Meter 662'2.1f?.Z0 (Yew No I Y2o TW4-25 .5g ,5i Flow I X" .o G P/V\ ~ No Meter 4z~on. L1o ~ No Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): -------------------------------- * Depth is measured to the nearest 0.01 feet. Monthly Depth Check Form Date !O /2. '-\I 2.D 1.3 Name --r;; ne• Ho} I ;J:j f Crc-r r ;" PC\.l!NVU Time Well Depth* Time Well Depth* tOO ] MW-4 ~r:s.gs O'l3'1 TWN-1 sc. 91 \00~ TW4-1 k,'-1·1.:; or.r~o TWN-2 31..\ I/ IDIO TW4-2 ~5 .'7'1 OCJifq TWN-3 3{;..70 1011 TW4-3 5'2. .I 0 Ot\'1b TWN-4 Yct.I.S 101i TW4-4 G/i.Cfl( 0'1~ TWN-7 87.'10 10l.l TW4-5 f.().Df. CitLJ~ TWN-18 ~g.7/ 100'1 TW4-6 b't .3 -z oq52. MW-27 sz.~o )00~ TW4-7 t.S .I ,S tOOD MW-30 75.21 1017.. TW4-8 bS.l( JDDY MW-31 ?,7.51 \O l'l TW4-9 57.75 0'1."3~ TW4-28 3/.D~ lOtS TW4-10 Sl.91 0~'-11 TW4-29 -rz...to 1014 TW4-11 S~tO oqSI TW4-30 -n. '5 D((~S TW4-12 '-\ L.. ')...., o"lS.'> TW4-31 ~). S1 OG\'11 TW4-13 L\i.S~ oq~Cf -tw~-3).. '-(~."Z.O Cl'\~ TW4-14 ~S.l\ C>'\SS 1\Jl.\-33 70.50 100~ TW4-15 «o3,b4 0 'IY1 -rwtf-3'i f,'f.IO }ODb TW4-16 bl.52 l 01 ~. ' TW4-17 ~~ 8b 013C. TW4-18 b I. b.j \Otl(,. TW4-19 b~.{;;f{ lot(, TW4-20 G,Z, bLf ol:\<.)'\ TW4-21 {.0 .'11.. IDI~ TW4-22 SfS, 15 lOc"Z. TW4-23 f,L\,t,':, !Ql\ TW4-24 IS .~~ Oj32-TW4-25 S'3:.. 'S C>g5!~ TW4-26 ~;3..00 0"\L!S TW4-27 8/.'Z'j Comments: (Please note the well number for any comments) * Depth is measured to the nearest 0.01 feet Weekly Inspection Form Date lp lu/,3 Svstem Ocerational (If no note Time Well De nth* Comments anv problems/corrective actions) _lo 1\ MW-4 73.17 Flow 4."( 6P.N". (Ye§) No Meter z. z3TZ.. '3 • Yo {fa~ No IVD7 MW-26 6'3.6l Flow I cJ . '1 6 P.,4A.. @]No Met.er 36~7 28'.54 (Ye~ No I o.z._6 TW4-19 2'1 ,L-ID Flow I Y.O() (YeS) No Meter J6't4l..3K.oe:.J ;r9§) No loo4 TW4-20 ,(2..51 Flow 10 .o h-P.M.. {Yes) No Meter 5'17YD5"97 ~No \o 1 4 TW4-4 7Cf. '18' Flow l·.5 (:, p ,/-"\.. (vev No Meter Z-05~80. fO ~No {)q'-10. I TWN-2 Zl,.So Flow I K .0 U./'--deS) No Meter l 1..\60 4 7. '23 ~s)No ()'15'1 TW4-22 51."7'l Flow HL~o.\ &P.I"'\.. ~No Meter 153'1,. 70_ (Ves No O_qSS TW4-24 £6. L{" Flow I fL I &P /"\ (Yej) No Meter 1.1 '-t'1D9 ~ oo (Yes) No - CJ CJ 45 TW4-25 52.77 Flow I,. £l &~.J.A.... C{e~No Meter ~32171. go (YeS) No Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): --------------- * Depth is measured to the nearest 0.01 feet. Weekly Inspection Form ( System Operational (If no note Time Well Depth* Comments anv nroblems/corrective actions} 13.5\ MW-4 6'l.<t( Flow 4.1.\ (,. p"""" (Yes~o Meter zz.ql ~o.38 ~Yes)No 134&-MW-26 {3. 3'-t Flow IO.I 6P./""\ (j__es) No Met.er 3'7166&.gl .. ~No ........ 1'--1 IS TW4-19 61. ~6 Flow I '-I . o 6-1' .-M. CYes) No Meter " l 7 26'"> b ::r. Q::: C{es)No LJ~5 TW4-20 62-65 Flow q,9 ('rf~ (~ No Meter s 'i gq z.o -1.5' ~No llS5 TW4-4 6'1.10 Flow ~. l &fl.,.,.. tfes) No Meter 'Z.1 o'-'·zt;. fO C(e~ No f.:U.S TWN-2 .Z.I.oZ. Flow tfLS &PA CiJW No Meter 1'-t~SI/, '-10 (Ye~ No It 4t.. TW4-22 .57.t1¥ Flow IS'· z. G-PY\. (YeS'} No Meter 7/3/l 30 (Yes) No 12.3<1 TW4-24 6£_2' Flow J7.Cf 6-PA (f_e_~ No Meter 6q39D.5. zo (res) No - 1330 TW4-25 6'L21 Flow 1g. o 6-P..M-(Yesj No Meter •··P-t2.Lt3L 3o 6e1> No Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): --------------- * Depth is measured to the nearest 0.01 feet. Weekly Inspection Form ( Date 11 J11 t,3 System Operational (If no note 1me W II e D er>th * c omments an:l£ (!roblems/corrective actions} \OOC) MW-4 6ct ~ z.~ Flow 4.'J C-f'M -~No Meter Z.344DI ~ Z5 {YeS) No - D'l57 MW-26 {3~8.5 Flow Ia .3 6-PA {Yesj No Met.er '373565 17 eYe~ No t120 TW4-19 60.yg-Flow I t--1,0 &P./A ~No Meter I 7.5 7 '2.$0 rn {res) No O'f54 TW4-20 ~?.30 Flow G). 9 G~,v... (Ye$) No Meter 600S.5Z.~z_ C1e$J No 106 '"{ TW4-4 6'1~-z.. Flow !f.o Grf _I.A.. tf_e]) No Meter '21506g, 40 ~No { D'U8 TWN-2 2"7 ~n Flow I S . 8' _G-P-""' Cf_e~ No Meter 1.53.63~ 2.0 ({e~ No O'l5o TW4-22 .5fL6D Flow I~ .o r .... PJ.A-tV~~ No Meter l Gl_i_''~j~ YD_ (Ye~ No _D_Cj"(6_ TW4-24 {3, 72_ Flow \ 8 .o &P.,...... (Ye~ No Meter 71L{I~'2 -~ &§J No D'l14 TW4-25 II. SO Flow i~.'-\ &P~ 6lesJ No Meter 'i5Z.372. 3'0 {fe~ No Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): --------------- * Depth is measured to the nearest 0.01 feet. ( ( Date i I ) 2.1 j z.o 1.::) Weekly Inspection Form Name -r:_,,.,~,.. HoJI ,·J~ Time Well Deoth* Comments nof. MW-4 Gtt "13 Flow i..l 3 Meter Z'-122 gq. Lt5 13o2. MW-26 Flow ,o.y 1·~ TW4-19 (.2.5~ Flow l"t.C Meter I Be let l$.o7 lZ.S~ TW4-20 b~.4z. Flow 10.0 Meter 602.'-1'-b.ZZ 1~11 TW4-4 7Lo3 Flow ~ D Meter 2'Z.lbLI7.o t2.4'-TWN-2 34.o1 Flow l~.b Meter ,.sgCJII. o TW4-22 Flow t~ o Meter ~lt:t71.5 I Z . .5'2. TW4-24 f,3:11 Flow rg'.o 1"2. '11 TW4-25 /O.Ob Flow 18.Y Operational Problems (Please list well number): System Operational (If no note any problems/corrective actions\ QeS)No - ~No (Ye~ No ( Ye~ No (Y~)No (Yes) No C'@S) No CveS) No (Y~No -eYe'S) No cY9s) No ~s)No CYe_§ No - (Yes) No Corrective Action(s) Taken (Please list well number): --------------- * Depth is measured to the nearest 0.01 feet. Weekly Inspection Form ( Date ,, fzs/,3 System Operational (If no note 1me Wll e D th* 91)1 c t ommen s bl I ti f ) an~ ~ro ems correc ve ac 1ons I ~L[(" MW-4 {p'f.s) Flow l.f,l/ t:A~ (Y~ No ., cr~ Meter ;l.4S"H~ .1/ No 1-;u 1 MW-26 ?2:~8'-Flow /0.~ "'"· ~s No oJ eve} No Met.er ~-:r:;03 z ""'i 14()/ TW4-19 (of."}-'if Flow ILl. 0 ~OuA. (res. No Meter ,!~~t~~~o~ (Yes 'No 1~1q TW4-20 (pf,'jj) Flow I ~ ~-... JD.1""' ~ No Meter l.,o~-2, 33 :1D I' (Ye)) No I 3 'If" TW4-4 ~Cf.t\.; Flow 'ff",o a.o-. ~No Meter ...,, (Y~ No "J-.1.!1-<. "'iii . 1.{ 0 1.328" TWN-2 -.2 7. Zl Flow 1 s.5 &P.,.cA (Yes\No Meter t61151. zo (Ye~ No 133~ TW4-22 s-9.n--Flow lt1/ r . .# .. ~ <Yes> No Meter ..,. ~No ~J..DloD,foD 1333 TW4-24 I L .l:J Flow I~ .0 &PJ.A {Yes) No Meter 7 S5S"Yb_."'] (Yes')No 1323 TW4-25 6'1.10 Flow j 9>. 7 6-f;V\. ~No Meter 41Zo2.2. 70 6'e8) No Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): --------------- * Depth is measured to the nearest 0.01 feet. Date il/z_o,j?,o\3 Monthly Depth Check Form Name -<nl\(..r ».II:J<\.r Time Well Depth* Time Well Depth* QI..S'S MW-4 b4 .iS ~bo~ TWN-1 .X.-iS ~ o(,!.c( TW4-1 (.j .OO QCol1 TWN-2 :!.~.15 ~bs.:!> TW4-2 b!..'li Qb:§J TWN-3 3b 70 ~~0_5,. TW4-3 Sl "'S Qk-'Z.'i TWN-4 L..j4 13 C>IO] TW4-4 10.0\ O"~j TWN-7 87."\1 O~Dl TW4-5 c;o.•HS' 0~'4'0 TWN-18 S.8. 7.& 070j TW4-6 £'!,53 Qt.30 MW-27 S'2..77 C>G..':.-{ TW4-7 'S.b.C. Ofsl) MW-30 7f;.,Z.C> ()701 TW4-8 f,S,Z.4 otn MW-31 b7· ,:SCl 6B!.}' TW4-9 .S~.Oj QIH{ TW4-28 3k>.q7 o1.S.~ TW4-10 ~~:lzs 0"135 TW4-29 1Z.!JJ ObSD TW4-11 S'6',:3j o7~fS TW4-30 -n.,-, Oil ~ TW4-12 112.32 07'10 TW4-31 fS3. 7..5 07'Z..'"l TW4-13 '17.1~ 07'-l IW '-\ -~'Z.. '1~.31 "IW'-1 .. ~~ .o~'-z:.c:. TW4-14 5.~ .Cfj 013:=:, -zo.s~ C>(:."\1 TW4-15 b3 ,q~ o1'3.t.. .,......, '-\ .. ~ \.j h'l ,151 C17S'i TW4-16 61 g~ 0750 TW4-17 I:!>.~S C>b03 TW4-18 (,).11 03JO TW4-19 b~.lS ()b"\~ TW4-20 ..58 .03 bt.IO TW4-21 61. 'i I o(,'\Z.. TW4-22 62. 73, 0107 TW4-23 b~. &'.S Sl(;~O TW4-24 ~ G~.~B Obl::l TW4-25 S1.'fj Cl i bC. TW4-26 (;;3)3 0710 TW4-27 [1,1.08 Comments: (Please note the well number for any comments) * Depth is measured to the nearest 0.01 feet Weekly Inspection Form Date Name ( System Operational (If no note Time We] Depth* Comments anllJ:!roblems/corrective actions) i JJ G MW-4 _6_~ z_q Flow 4.'-\ b-PAA (i~ No Meter '250611.5'-t ~S.) No 1315 MW-26 63. 'lO Flow \0.0 &PM tfes) No Met.er 3lS6DCl,5~ ~No 151>" TW4-19 6q. '-f':f_ Flow I '-t .Oo (Yes )No Meter \8S:oc 6-.:. . "iu (Ye?) No 13iZ TW4-20 7Z.Il5 Flow 9~1 &_PA cJes) No Meter 6o L.lgll~.6o (fe~ No . IJ 2.3' TW4-4 6'1.66 Flow $5 " 6-r.M ?fes)No Meter Z. Z8't~~. '-to ~No ( \"l.3'2.. TWN-2 '2..6 70 Flow lg 6 ~P#\ {YeS' No cf{e~ Meter I b~Ot.!ll ~D No 170'( TW4-22 s~ ~~-. Flow IS.O GPI"\ {Ye~ No Meter B4o€.0 . So {feS) No _, 1305 TW4-24 '71. 20 Flow 1-L L.l 6-P,..v\ (Yes') No Meter 115631. '-'0 eYes No 122.._1\ TW4-25 fi(J .DO Flow j(_g &r...v\.. «e§) No Meter Ligz. 7 35 ._'\0 ~.No Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): --------------- * Depth is measured to the nearest 0.01 feet. \ \ Date ~~~ "1/zo 13 Tl me W II e D th* ep1 1'32.0 MW-4 C.~.cl ~ 1317 MW-26 (:.l{.~O ~ TW4-19 "8-1~ l'31S TW4-20 7Z. B_j I'~L'> TW4-4 (/i.~3 l'30S TWN-2 z.'-..60 131C TW4-22 5~.:.10 \~0'1 TW4-24 '10.03 \3C( TW4-25 61.60 Weekly Inspection Form Name ~r y,,);)'\3 System Operational (If no note c t ommen s bl I ti tl ) anl! ero ems correc ve ac ons Flow 4.3 eYes )'Jo Meter -z..sc.o 81· 2.3 C'Yes)No Flow 10'~ CYesJ No Met.er "3$0C:: 1~.~ (YeS) No Flow )LLO C:Yes) No Meter l'Z7CJ'3 L\1. o7 CYe~ No . ......., Flow !D.O (Ye~ No Meter 60bZ.6.7 gg ~No - Flow 1,'-4 (YeS) No Meter 2.33..5>~1.4 _Cvev No Flow 15.0 eYes) No Meter \6~1 £S,q (ves.-,\No - Flow 16:5 ~vevNo Meter "!;f> 711:> :o C:Yes~o Flow ~ 16.9 c_Yei)No Meter 7~ (, \~Z., g ('Yes) No Flow \(.0 (YesJNo Meter 49Z780 .D Q'e:W No Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): -------------- " Depth is measured to the nearest 0.01 feet. Weekly Inspection Form ( Date ,zjl(:,/z..6D Name ~v-n"v-1-}PJ/,)j Svstem Ooerational (If no note Time Well Deoth* Comments anv problems/corrective actionsj JL{{O MW-4 b'L03 Flow 4,3 ~)No Meter Z.G.J3S l.z. \ c:Yes) No )~Ob MW-26 ""' .'1~ Flow ~IO·Z c-v-es)No Met.er 3524S""I, ~.3 ( Yes~o 1~2.1 TW4-19 G:.7.1S Flow 11-J.D ~Y~No Meter l'iO (, 7 4 0. OY (YeS) No ~ lil>3 TW4-20 "71 .~~ Flow 10.0 (Yes ~o Meter f:,077 '-lo 70 cYes~No 1~13 TW4-4 b~.1~ Flow /,g -, ....._ C Yes l')o Meter z:>~ \ ~'1· b (Yes )No - l"':l55 TWN-2 31.), DES Flow \g.o CYes)No Meter nz.so~. g ( Ye$! No J!.jOO TW4-22 S1,~1 Flow 1&.'~ c Y~No Meter ~$797.3 C__ve§:)No 1]57 TW4-24 6L1,17 Flow 17. '1 ~YeS) No Meter ~162Db. \ C YeuNo J).SD TW4-25 63.1 Flow 11."3> ~s_) No Meter ~oz..GHD Cvesj No Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): --------------- ( * Depth is measured to the nearest 0.01 feet. Weekly Inspection Form Date rz./z3 /2DI3 Name ...,-;;::.,f)(:(" ~" 11.'J.j System Operational (If no note T' 1me W II e 0 th"' .eP' c t ommen s bl I i i ) an)£ ero ems correct ve_ act ons IY3'1 MW-4 b'f.8S Flow Y.3 C Yes)No Meter 7...b'7 ~b. 70 (_ ve~~No .... 142.q MW-26 6 7.:3'S Flow 10 ~ C~No Met.er 38'L..j~8lS'.~o ( Yes )\Jo 1 G'5l' TW4-19 £Y). lrJ Flow lY .O (Yes)No l~.SO Meter ·,9 ·:nss'i .0-t, (Yes __:No \111.::, TW4-20 /Z.Y'i Flow lD 0 l(Eis ~o Meter 60c.tz_2g .f.b C Yes ) No ~~ TW4-4 6q.qs Flow 1.~ C-ygs "No ''n'1 Meter '2..'-\~1'1\.7 (Yes) No -- ( \Lil'l TWN-2 3'l.. 0 'i Flow~ 1~.0 ~s~o Meter \76.300.2 LVeS\ No \~lD TW4-22 e:,O.oo Flow 1~.5 ("Y~s)No Meter lf6.h$0 ,1 (Yes)No - IL.\ 11 TW4-24 "Lt' 7.3 Flow ~ \1.~ /Y_es'f'Jo Meter ~37~gq,9 >< X c._ nJS )No I~DB TW4-25 b~.C>l Flow \7,.5 (Yes)No Meter SOb.'\59.3 C_VeS)No - Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): --------------- * Depth is measured to the nearest 0.01 feet. 40G/1U Weekly Inspection Form System Operational (If no note T' tme W II e D h* ept c omments bl I . . ) anl£1!ro ems correct ave .actaons 12'-17 MW-4 /,9_5o Flow S.3 6-PA (19~ No Meter 27Z'i3z.sg eYe~ No IZ_51 MW-26 A5 31? Flow I 0. t1 &¥.).A. (YeS) No Met.er 386531.50 (Ye~ No - 1350 TW4-19 /(7 gy-Flow 14 .a ~P.I-A. C[eS) No Meter 'q~?L{2.~8'-~ ~JNo j3DD TW4-20 7'i 5.3 Flow I~-o 6-i='...N\. ~No Meter .<IO~Dl 51 <Ye5J No IZ4"\ TW4-4 t(q .'io Flow ~LD 6-j:>~ Ciii?) No Meter 2"i S'06'i. zo <Y_eS) No ( L3l0 TWN-2 31. 7L.{ Flow 13.3 G?~ (Yes) No Meter I tgo6DS. 10 (Ye~ No 1~5 TW4-22 5'Lh Flow lll. 0 6-P ..-v\.. Cfes) No Meter t.i27'i.5-70 ~No 11DQ TW4-24 go.o Flow I~ 0 &PA (Yes\ No Meter f6oi.OA. 11"1 • 10 C(e~No 13zS TW4-25 AO 7R Flow I 8'.~ 6-P./V\. {YeS\ No Meter .c; jq£:)'17 7[) (Yes) No Operational Problems (Please list well number): Corrective Action(s) Taken (Please list well number): --------------- ( * Depth is measured to the nearest 0.01 feet. @ estimated dry area MW-5 perched monitoring well showing e sso3 elevation in feet amsl TW4·22 temporary perched monitoring well 0 5582 showing elevation in feet amsl lWN-7 h d . .t . .A5562 temporary perc e nitrate mom onng V well showing elevation in feet amsl PIEZ-1 perched piezometer showing Q 5592 elevation in feet amsl TW4-32 temporary perched monitoring well ~ 5564 installed September, 2013 showing approximate elevation in feet amsl RUIN SPRING & 5380 seep or spring showing elevation in feet amsl NOTE: MW-4, ~W-26. TW4-4. TW4-19. and 1W4-20 are chlorolorm HYDRO GEO CHEM,INC. KRIGED 4th QUARTER, 2013 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE FI<!YRE c -1 H :/718000/feb14/Uwl1213.srf ' ,. ,, estimated nitrate capture zone boundary stream tubes resulting from pumping estimated chloroform capture zone boundary stream tubes resulting from pumping @ estimated dry area MW-5 perched monitoring well showing e 5503 elevation in feet amsl rw0 4-12 temporary perched monitoring well 5582 showing elevation in feet amsl TW~ hed " .. <>5562 temporary perc mtrate monltonng well showing elevation in feet amsl PIE2·1 perched piezometer showing Q 5592 elevation in feet amsl TW4-32 temporary perched monitoring well 3::t 5564 installed September, 2013 showing approximate elevation in feet amsl RUIN SPRING ~ 5380 seep or spring showing elevation in feet amsl HYDRO GEO CHEM,INC. APPROVED ~Oil~ ~11 KRIGED 4th QUARTER, 2013 WATER LEVELS AND ESTIMATED CAPTURE ZONES WHITE MESA SITE DATE REFERENCE H:/718000/feb14/ nitrate/Uwl1213cz2nt.srf FIGURE C-2 .,. .. estimated nitrate capture zone boundary stream tubes resulting from pumping ," " I I MW-4 e sss3 TW4-1 0 5554 PIEZ-2 Q 5595 TW4-32 ~S564 estimated chloroform capture zone boundary stream tubes resulting from pumping perched monitoring well showing elevation in feet amsl temporary perched monitoring well showing elevation in feet amsl perched piezometer showing elevation in feet amsl temporary perched monitoring well installed September, 2013 showing elevation in feet amsl 554() 5535 ss3o NOTE: MW-4, MW-26, TW4-4, TW4-19, and TW4-20 are chloroform pumping wells; TW4-22, TW4-24, TW4-25, and TWN-2 are nitrate pumping wells HYDRO GEO CHEM, INC. KRIGED 4th QUARTER, 2013 WATER LEVELS AND ESTIMATED CAPTURE ZONES WHITE MESA SITE DATE nitrate/U1213cznt.srf TabD Kriged Previous Quarter Groundwater Contour Map @ estimated dry area MW-5 perched monitoring well showing e 5503 elevation in feet amsl rw0 4·12 temporary perched monitoring well 5582 showing elevation in feet amsl TWN-7 h d . . . A.5562 temporary perc e mtrate momtonng V well showing elevation in feet amsl PIEZ-1 perched piezometer showing tiil 5593 elevation in feet amsl TW4-32 temporary perched m01.1itqrlng well ~ 5564 installed September. 2013 showing approximate elevation in feet amsl RUIN SPRING b 5380 seep or spring showing elevation in feet amsl NOTE: MW-4. MW-26; TW44. TW4-19, and TW4-20 are ch1oroform HYDRO GEO CHEM,INC. KRIGED 3rd QUARTER, 2013 WATER LEVELS WHITE MESA SITE "Pi'ROVEll DATE REFERENCE FIGURE H:/718000/nov13/Uwl0913.srf I D-1 TabE Hydrographs of Groundwater Elevations Over Time for Nitrate Monitoring Wells -....! 0 0 0> 0 0 Depth Below Measuring Point (ft.) (]1 0 0 • ~ ~ • ~ 9 0 (,.) 0 0 I 1\) 0 0 ' 0 0 I 0 0 . 06/01/08 12/18/08 07/06/09 01/22/10 08/10/10 02/26/11 09/14/11 04/01/12 10/18/12 05/06/13 11/22/13 06/10/14 -4 :e z I ...... ~ -C'D ""'': r C'D < !. 0 < C'D ""'': ::t 3 C'D -= . 2: 3 "C - w 01 0 Depth Below Measuring Point (ft.) w 0 0 1\) 01 0 / v • -- 1\) 9 0 ..... 01 0 T ) ~~ N ~ v I t r" / -· ·---~ -- ..... 0 0 - 01 0 0 0 . 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Q) ~ ~/9G/G0 -as 3: (0 I z ~ 0~/0~/BO 0~/GG/~0 60/90/LO BO/B ~/G ~ +----+-----l------+------+----f----------1 CD !l> 0 .... CD 0'> 0 Depth Below Measuring Point (ft.) ~ 0 CD 1\) 0 I CD 0 0 \ 1 \ ) 4( \ t ~ CXl CXl 0 ~\ ~ ~ CXl 0'> 0 . - --~ ------~ 12/18/08 07/06/09 01/22/10 08/10/10 ~ z I ....... ~ 02/26/11 -(D ""'l r (D < ~ 09/14/11 0 < (I) ""'l ::! 3 04/01/12 (I) -~ 2: 3 'tJ 10/18/12 - 05/06/13 11/22/13 06/10/14 0> w a, 0> w ~ Depth Below Measuring Point (ft.) 0> w i\l 0> w 0 ~ 0> ..__ ---. ~~ 0> 1\) "' 0> 1\) ~ 0> 1\) i\l ~~ ~ • ( ~ \ ~ 0 ""'-. 0> ...... 0> ' I ~ ~ ....-- 0> _. a, 07/06/09 01/22/10 08/10/10 ~ 02/26/11 z I ...... ~ :e m -(1) """ . 09/14/11 r-(1) < !!!.. 0 < (1) . 04/01/12 """ ::! 3 (1) -:= . 10/18/12 2: 3 "C - 05/06/13 11/22/13 06/10/14 p ~10 ~/90 .-----..-----..,...-----...-----,---------, £~/90/90 -a. E -c: ~/8 ~/0 ~ .c ..: --Q) E i= C:~/W/PO a.. Q) > 0 a; > Q) ..J ~ ~/P~/60 · a.. Q) -ca 3: (D ,... I ~ ~/9C:/C:O z ~ 0~/0~/80 60/90/LO -1------+-----+------l-------l---------l -0. E :a . ---Q) E ;:: ~ Q) > 0 Gi > Q) ..J ~ Q) -m 3: co ~ I z ~ v~!0~/90 £~/90/SO ~~/B~/0~ ~~/W/vO ~ ~/v ~/60 ~ ~/9~/~0 0~/0~/BO 0~1~~/W 60/90/LO - 0 0 0 0 ,.... 0 0 C\1 0 0 (") r ~ ~ ~ ~ ~~ +::::: r----_ 1---.. 0 0 "<t ~ .c: v 1-----. 0 0 10 (.}1 (.}1 Ot ~ 0 Depth Below Measuring Point (ft.) (.}1 ~ Ot (.}1 ~ 0 (.}1 c:.u Ot (.}1 c:.u 0 (.}1 1\) Ot (.}1 1\) 0 1-----+----l----1----+----f-----t----t-07/06/09 01/22/10 08/10/10 02/26/11 09/14/11 . 04/01/12 10/18/12 -05/06/13 11/22/13 I 06/10/14 ~ z I ..... CD ~ -C'D ""'1: .... C'D [ 0 < C'D ""'1: ::1 3 C'D -:= 2: 3 "C - ..-. a. E -.c . ... ,..... -Cl) E ·-1-... Cl) > 0 -Cl) > Cl) ..J ... Cl) ... ~ 0 (W) I 3: ~ v ~/Lc/c ~ -·.------.--------.------,------,------.--------, £ ~~v~/80 c~/W/vO 0~/8~H ~ • 60/90/LO - 80/cc/cO ~ 90/0 ~/0~ 90/8c/90 +-----+------+-----+------1------4-------l 0 lO ,..... 0 o:i ,..... 0 0 <X) -c. E -.c . .... .... -CD E ·-1- llooo CD > 0 -CD > CD ...J llooo CD .... ca ~ ,.. M I ~ := v~/Lc/U £ ~~v~/80 G~/W/vO 0~/8~/~~ 60/90/LO 80/GG/GO 90/0~/0~ S0/8c/SO - - - 0 <ci co ; ~ \ ~ ~ 0 a:i co f ~ ) .~ 0 0 I'- ~l.-----L--- ~ l.-----1--- 0 a:i I'- C! 0 co TabF Depths to Groundwater and Elevations Over Time for Nitrate Monitoring Wells Water Levels and Data over Time White Mesa Mill -Well TWN -1 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5,646.96 5,648.09 1.13 112.5 5,600.38 02/06/09 47.71 46.58 5,599.99 07/21/09 48.10 46.97 5,600.26 09121109 47.83 46.70 5,601.10 10/28/09 46.99 45.86 5,602.59 12/14/09 45.50 44.37 5,600.55 03/11/10 47.54 46.41 5,600.66 05/11/10 47.43 46.30 5,599.18 09/29/10 48.91 47.78 5,598.92 12/21/10 49.17 48.04 5,598.29 02/28/11 49.80 48.67 5,597.80 06/21/11 50.29 49.16 5,597.32 09/20/11 50.77 49.64 5,597.15 12/21/11 50.94 49.81 5,596.54 03/27/12 51.55 50.42 5,596.52 06/28112 51.57 50.44 5,595.03 09/27/12 53.06 51.93 5,596.62 12/28/12 51.47 50.34 5,593.54 03/28/13 54.55 53.42 5,592.38 06/27113 55.71 54.58 5,591.65 09/27/13 56.44 55.31 5,590.34 12/20113 57.75 56.62 Water Levels and Data over Time White Mesa Mill-Well TWN-2 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitorin8 (blw.MP) (blw.LSD) Well 5,625.75 5,626.69 0.94 95 5,611.37 02/06/09 15.32 14.38 5,610.63 07/21109 16.06 15.12 5,609.73 09/21109 16.96 16.02 5,607.08 11/02/09 19.61 18.67 5,606.57 12/14/09 20.12 19.18 5,612.45 03/11110 14.24 13.30 5,612.78 05111110 13.91 12.97 5,611.37 09/29/10 15.32 14.38 5,610.24 12/21110 16.45 15.51 5,610.64 02/28/11 16.05 15.11 5,609.78 06/21/11 16.91 15.97 5609.79 09/20111 16.90 15.96 5609.72 12/21/11 16.97 16.03 5,605.69 03/27/12 21.00 20.06 5,605.67 06/28/12 21.02 20.08 5,603.03 09/27/12 23.66 22.72 5,605.76 12/28112 20.93 19.99 5,598.28 03/28113 28.41 27.47 5,594.32 06/27113 32.37 31.43 5,594.38 09/27/13 32.31 31.37 5,594.68 12/20/13 32.01 31.07 Water Levels and Data over Time White Mesa Mill -Well TWN -3 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5,633.64 5,634.50 0.86 110 5,603.77 02/06/09 30.73 29.87 5,602.37 07/21109 32.13 31.27 5,602.34 09/21/09 32.16 31.30 5,602.60 10/28/09 31.90 31.04 5,603.12 12114/09 31.38 30.52 5,602.90 03/11/10 31.60 30.74 5,603.23 05111110 31.27 30.41 5,602.86 09/29/10 31.64 30.78 5,603.35 12/21110 31.15 30.29 5,602.89 02/28111 31.61 30.75 5,602.75 06/21111 31.75 30.89 5,602.40 09/20111 32.10 31.24 5,602.40 12/21111 32.10 31.24 5,601.70 03/27/12 32.80 31.94 5,601.67 06/28/12 32.83 31.97 5,600.50 09/27/12 34.00 33.14 5,601.74 12/28112 32.76 31.90 5,598.60 03/28/13 35.90 35.04 5,597.18 06/27/13 37.32 36.46 5,597.36 09/27/13 37.14 36.28 5,597.60 12/20/13 36.90 36.04 Water Levels and Data over Time White Mesa Mill -Well TWN -4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,641.04 5,641.87 0.83 136 5,601.47 02/06/09 40.40 39.57 5,604.26 07/21109 37.61 36.78 5,605.02 09/21109 36.85 36.02 5,605.87 10/28/09 36.00 35.17 5,605.81 12/14/09 36.06 35.23 5,605.31 03/11110 36.56 35.73 5,605.36 05/11/10 36.51 35.68 5,604.59 09/29110 37.28 36.45 5,604.42 12/21110 37.45 36.62 5,603.69 02/28/11 38.18 37.35 5,603.36 06/21111 38.51 37.68 5,602.82 09/20/11 39.05 38.22 5,602.79 12/21111 39.08 38.25 5,600.82 03/27112 41.05 40.22 5,600.84 06/28/12 41.03 40.20 5,598.47 09/27/12 43.40 42.57 5,600.86 12/28/12 41.01 40.18 5,595.57 03/28/13 46.30 45.47 5,594.12 06/27/13 47.75 46.92 5,593.33 09/27/13 48.54 47.71 5,591.92 12/20/13 49.95 49.12 Water Levels and Data over Time White Mesa Mill-Well TWN-6 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5,663.03 5,664.94 1.91 135 5,589.52 08/25/09 75.42 73.51 5,589.46 09/22/09 75.48 73 .57 5,589.61 11/03/09 75.33 73.42 5,589.92 12114/09 75.02 73.11 5,590.24 03/11110 74.70 72.79 5,590.40 05111110 74.54 72.63 5,590.24 09129110 74.70 72.79 5,590.49 12/21110 74.45 72.54 5,590.16 02/28111 74.78 72.87 5,590.44 06/21111 74.50 72.59 5,590.35 09/20/11 74.59 72.68 5,590.67 12/21111 74.27 72.36 5,590.34 03/27/12 74.60 72.69 5,590.32 06/28/12 74.62 72.71 5,589.77 09/27112 75.17 73.26 5,589.67 12/28/12 75.27 73.36 5,589.45 03/28113 75.49 73.58 5,589.01 06/27/13 75.93 74.02 5,588.99 09/27/13 75.95 74.04 5,588.15 12/20/13 76.79 74.88 Water Levels and Data over Time White Mesa Mill -Well TWN -7 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,647.39 5,649.26 1.87 120 5,552.56 08/25/09 96.70 94.83 5,558.34 09/21/09 90.92 89.05 5,558.82 11110/09 90.44 88.57 5,558.96 12114/09 90.30 88.43 5,559.54 03/11/10 89.72 87.85 5,559.60 05/11110 89.66 87.79 5,559.83 09/29110 89.43 87.56 5,559.00 12/21/10 90.26 88.39 5,559.68 02/28111 89.58 87.71 5,560.43 06/21111 88.83 86.96 5,560.46 09/20/11 88.80 86.93 5,560.78 12/21111 88.48 86.61 5,560.92 03/27112 88.34 86.47 5,560.87 06/28/12 88.39 86.52 5,561.40 09/27112 87.86 85.99 5,561.50 12/28/12 87.76 85.89 5,562.01 03/28113 87.25 85.38 5,562.21 06/27113 87.05 85.18 5,562.41 09/27113 86.85 84.98 5,562.23 12/20/13 87.03 85.16 Water Levels and Data over Time White Mesa Mill-Well TWN-14 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5,647.80 5,649.53 1.73 135 5,586.18 11/04/09 63.35 61.62 5,586.51 12/14/09 63.02 61.29 5,586.71 03111110 62.82 61.09 5,586.72 05/11/10 62.81 61.08 5,586.53 09/29/10 63.00 61.27 5,586.80 12/21110 62.73 61.00 5,586.74 02/28111 62.79 61.06 5,586.84 06/21111 62.69 60.96 5,586.73 09/20/11 62.80 61.07 5,586.98 12/21111 62.55 60.82 5,587.07 03/27/12 62.46 60.73 5,587.10 06/28/12 62.43 60.70 5,587.07 09/27112 62.46 60.73 5,587.33 12/28/12 62.20 60.47 5,587.43 03/28113 62.10 60.37 5,587.43 06/27113 62.10 60.37 5,587.72 09/27113 61.81 60.08 5,587.22 12/20/13 62.31 60.58 Water Levels and Data over Time White Mesa Mill-Well TWN-16 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,651.07 5,652.70 1.63 100 5,603.34 11/04/09 49.36 47.73 5,603.56 12114/09 49.14 47.51 5,603.84 03111110 48.86 47.23 5,604.31 05/11110 48.39 46.76 5,604.28 09129110 48.42 46.79 5,604.39 12/21110 48.31 46.68 5,604.20 02/28/11 48.50 46.87 5,604.55 06/21/11 48.15 46.52 5,604.74 09/20/11 47.96 46.33 5,604.94 12/21111 47.76 46.13 5,604.84 03/27/12 47.86 46.23 5,604.85 06/28112 47.85 46.22 5,604.99 09/27112 47.71 46.08 5,605.10 12/28/12 47.60 45.97 5,605.22 03/28113 47.48 45.85 5,605.11 06/27/13 47.59 45.96 5,605.39 09/27113 47.31 45.68 5,604.99 12/20/13 47.71 46.08 Water Levels and Data over Time White Mesa Mill -Well TWN -18 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,643.95 5,645.45 1.50 100 5,586.85 11102/09 58.60 57.10 5,600.14 12114/09 45.31 43.81 5,587.36 03/11/10 58.09 56.59 5,587.71 05111110 57.74 56.24 5,587.50 09129110 57.95 56.45 5,607.66 12/21/10 37.79 36.29 5,587.35 02/28/11 58.10 56.60 5,587.71 06/21111 57.74 56.24 5,587.65 09/20/11 57.80 56.30 5,587.95 12/21111 57.50 56.00 5,587.05 03/27112 58.40 56.90 5,587.05 06/28/12 58.40 56.90 5,587.50 09/27/12 57.95 56.45 5,587.50 12/28/12 57.95 56.45 5,587.32 03/28/13 58.13 56.63 5,586.95 06/27/13 58.50 57.00 5,587.02 09/27/13 58.43 56.93 5,586.26 12/20/13 59.19 57.69 Water Levels and Data over Time White Mesa Mill -Well TWN-19 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,659.59 5,661.36 1.77 110 5,606.17 11102/09 55.19 53.42 5,606.70 12/14/09 54.66 52.89 5,607.22 03111110 54.14 52.37 5,607.89 05/11110 53.47 51.70 5,607.98 09/29/10 53.38 51.61 5,608.41 12/21110 52.95 51.18 5,608.49 02/28111 52.87 51.10 5,608.60 06/21/11 52.76 50.99 5,609.17 09/20/11 52.19 50.42 5,608.90 12/21111 52.46 50.69 5,608.87 03/27/12 52.49 50.72 5,608.86 06/28/12 52.50 50.73 5,608.86 09/27112 52.50 50.73 5,608.86 12/28/12 52.50 50.73 5,609.17 03/28/13 52.19 50.42 5,608.88 06/27/13 52.48 50.71 5,608.92 09/27/13 52.44 50.67 5,608.46 12/20/13 52.90 51.13 Water Levels and Data over Time White Mesa Mill -Well MW -30 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitorin~ (blw.MP) (blw.LSD) Well 5 61 3.34 5 614.50 1.16 110 5,534.92 10/24/2006 79.58 78.42 5,535.09 3/16/2007 79.41 78.25 5,535.46 8/27/2007 79.04 77.88 5,535.06 10115/2007 79.44 78.28 5,535.78 3115/2008 78.72 77.56 5,536.26 6/15/2008 78.24 77.08 5,536.35 9/15/2008 78.15 76.99 5,536.68 11115/2008 77.82 76.66 5,535.42 3115/2009 79.08 77.92 5,537.11 6/30/2009 77.39 76.23 5,536.93 9110/2009 77.57 76.41 5,537.23 12/11/2009 77.27 76.11 5,537.59 311112010 76.91 75.75 5,537.85 511112010 76.65 75.49 5,538.37 9/29/2010 76.13 74.97 5537.70 12/21/2010 76.8 75.64 5537.67 2/28/2011 76.83 75.67 5538.31 6/21/2011 76.19 75.03 5538.15 9/20/2011 76.35 75.19 5538.42 12/21/2011 76.08 74.92 5538.54 3/27/2012 75.96 74.8 5538.60 6/28/2012 75.9 74.74 5538.68 9/27/2012 75.82 74.66 5538.99 12/28/2012 75.51 74.35 5539.25 3/28/2013 75 .25 74.09 5539.05 6/27/2013 75.45 74.29 5539.60 9/27/2013 74.90 73.74 5539.67 12/20/2013 74.83 73 .67 Water Levels and Data over Time White Mesa Mill-Well MW-31 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,615.26 5,616.40 1.14 130 5,544.07 10/24/2006 72.33 71.1 9 5,544.45 3116/2007 71.95 70.81 5,536.94 8/27/2007 79.46 78.32 5,544.62 10115/2007 71.78 70.64 5,545.37 3115/2008 71.03 69.89 5,544.50 6/15/2008 71.90 70.76 5,545.94 9/15/2008 70.46 69.32 5,546.42 11115/2008 69.98 68.84 5,546.03 3/15/2009 70.37 69.23 5,546.65 6/30/2009 69.75 68.61 5,546.45 9110/2009 69.95 68.81 5,546.75 12/1112009 69.65 68.51 5,547.09 3/1112010 69.31 68.17 5,547.41 5111/2010 68.99 67.85 5,547.28 9/29/2010 69.12 67.98 5547.45 12/2112010 68.95 67.81 5547.37 2/28/2011 69.03 67.89 5547.96 6/21/2011 68.44 67.3 5547.65 9/20/2011 68.75 67.61 5548.34 12/2112011 68.06 66.92 5548.30 3/27/2012 68.10 66.96 5548.40 6/28/2012 68.00 66.86 5548.59 9/27/2012 67.81 66.67 5548.91 12/28/2012 67.49 66.35 5549.14 3/28/2013 67.26 66.12 5548.90 6/27/2013 67.50 66.36 5549.25 9/27/2013 67.15 66.01 5549.16 12/20/2013 67.24 66.10 TabG Laboratory Analytical Reports INORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. 4th Quarter Nitrate 2013 1310396-010 Client Sample ID: Piez-01_10162013 ANA L v r1 c AL LAs oRAro R' f s Collection Date: 10116/2013 1105h 463 West 3600 South Received Date: 10118/2013 1 OOOh Analytical Results Compound Units Date Prepared ;alt Lake City, UT 84115 Chloride mg!L Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Nitrate/Nitrite (as N) mg/L Date Analyzed 10/21/2013 235111 10/22/2013 205911 Contact: Garrin Palmer Method Used E300.0 E353.2 Reporting Limit 10.0 1.00 Analytical Result 54.1 6.68 Qual Report Date: I 0/2912013 Page 13 of20 All analyses applicable totlle CWA. SDWA. and RCRA are rcrformcd in accordance to NEL\C pro1oc:ols. Per1incnt sampling inFonnalion is localed on 1h~ attached COC Confidential Busincs.·~ lnfomtation: This report is pruYitk--d for the exclusiYe usc of the ::,&Jn.'SS\.'C. Pri\ile~cs o~su~c-q~cnt ~c of the "~'?c ofthis.cm~))\UlY or any ~mbcr of its staff. orn.Jlroducti~ ~flhis £ql0~ in ~on!"-'Ction .. \\ilh the ~\'crliscnl\.:nl, p~omotio_n or sale of~~}:~rod~t or p~~ ~r in ~nnt.;~on \\~tb t~ n;-puhlica.tion oflhls n:port INORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. 4th Quarter Nitrate 2013 1310396-011 Client Sample ID: Piez-02_10162013 ANAl vr1 cAl lAB o RAreR, E s Collection Date: 10/16/2013 1010h Received Date: Analytical Results 463 West 3600 South Compound ~alt Lake City, UT 84115 Chloride 10/18/2013 1 OOOh Units Date Prepared Nitrate/Nitrite (as N) mg/L mg/L Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QAOfficer Date Analyzed I 0/22/20 13 00 14h I 0/22/20 13 2100h Contact: Garrin Palmer Method Used E300.0 E353.2 Reporting Limit 5.00 0.100 Analytical Result 9.22 0.364 Qual Report Date: 10/29/2013 Page 14 of20 All ann lyses applicable to the CWA. SOW A. and RCRA are rcrfonncd in accordance to NELAC protocols. Pertinent sampling inronnation is located on the attached COC Confidential Business lnformalion: This report is proYidct.l for the exclusive l..L'iC uflhe ~dd~-c. Privileges ofsuhsequ...'111. ~of the ~~~c of this .company or any ~'1Tllx'T ofils staff, or reproducll~ ~fthis report in connection~ '\ilh the ~:cr11semcnt. p~motio_n or sale of any~~~ or ~occss, ~r in ~onru..'Ciion with th; ~-publication of this n.--port INORGANIC ANALYTICAL REPORT 463 West 3600 South Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. 4th Quarter Nitrate 2013 1310396-012 Client Sample ID: Piez-03_10162013 Collection Date: 10/16/2013 1035h Received Date: Analytical Results Compound 10/18/2013 lOOOh Units Date Prepared ~alt Lake City, UT 84115 Chloride mg!L mg!L Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (801)263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QAOfficer Nitrate/Nitrite (as N) Date Analyzed I 0/22/20 J 3 003 7h 10/22/2013 2101h Contact: Garrin Palmer Method Used E300.0 E353.2 Reporting Limit 5.00 0.100 Analytical Result Qual 23.5 1.80 Report Date: 10/29/2013 Page 15 of20 All am lyses applkabl!! h> tht: CWA, SDWA. and RCRA arc p:rrnnncd in accordance to NELA.C protocols. Pertinent sampling infonnation i.'i Jocatl!d on the an.achcd COC. Contltkntial BusiltC$S lnfom1ation: This report is prm;ded t'in the C:(CI~l-..·~ use of the ~tldrcs.."t.-c Pri,·ile~cs o[sub;r;;cq~nt ~~oft he n~~n.: ofthi\con;p."lny or any r:mtx,-of its slaff. or r-eprotluctlon ~this ~ in ;on~ction .... \\ilh the ~\·crtisc~t. p~omotio.n Ol"salc of~~ ~00~ or ~-ss, ~r in ~'tl~~ic'tl with the r:,-publication of this n.--port 463 West 3600 South ;alt Lake City, UT 84115 Phone: (80 l) 263-8686 Toll Free: (888) 263-8686 Fax: (80 l) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 4th Quarter Nitrate 2013 Lab Sample ID: 13103 96-002 Client Sample ID: TWN-01_10162013 Collection Date: 10116/2013 0727h Received Date: 10118/2013 lOOOh Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Chloride mg/L 10/21/2013 1606h E300.0 5.00 26.8 Nitrate/Nitrite (as N) mg/L 10/22/2013 2103h E353.2 0.500 1.61 Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of the previously issued reports. Qual Report Date: I 0/30/20 13 Page 5 of 20 All analyse..o; applicable to the CWA. SDWA. and RCRA are performed in accorJ.anc:e to NELAC protocols. Pertinent sampling information is localct.1 on the attached COC_ Confidcr1tiol Busint.~ Jnfomlation: This report is pro"idcd for the cxclusin usc of the ~ddn.--sscc. Prh·ilc~cs o! sub,scq~nt ~of the ~~~c of this con:'pany or any ~'T.nhcr of irs s1aff. or rcproduct~ ~~this rcpo~ in ~on~cction, y,;lh the ~~cr1iscmcn1, ~omoli~ or sale uf ~ny ~rodu.ct or p~occss, ~r in ~onn~c!ion w!lh I he r~-publicalion of 1his n.-por1 American West ANAlYTICAl LABORATORIES 463 West 3600 South )alt Lake City, UT 84115 Phone: (801) 263-8686 roll Free: (888) 263-8686 Fax: (80 1) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 4th Quarter Nitrate 2013 Lab Sample ID: 1310396-006 Client Sample ID: TWN-02_10162013 Collection Date: 10/16/2013 0950h Received Date: 10/18/2013 1 OOOh Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Chloride mg!L 10/21/2013 2022h E300.0 10.0 70.4 Nitrate/Nitrite (as N) mg/L 10/22/2013 2108h E353.2 10.0 111 Reissue of a previously generated report. Information has been added, updated, or revised Information herein supersedes that of the previously issued reports. Qual Report Date: 10/30/2013 Page 9 of20 All amlyses applicable lo lhe C\\'A SDWA. and RCR.~ are ("M.."rfOmk---d in ~cordancc-to NELAC protocols Pcrtimmt sampling infonnalion is locatctl un the ttH;:~chcd COC, Con1idcntial Business Lnfonmtlion: Thi.s n:port is pnnidcd for the exclusiv.;: usc of the ~dd~-c. Prh ilc~cs orsub~seq~L'Tlt t~ uflhc ~~cor this 4con:pany or any ~""DlhL'T ofils staff, or rcproductio~ ?.~this r\.'(K'~ in ~on~ccliun_. \\ith the ~~crtiscn.'M!nl. p~motio_n ~r o:;alc of~~· ~l~l or ~css, ~r in :'"m'";_--c~ion w!lh lh~ ':-p~blicalion ol this rqx-.rt 463 West 3600 South ~alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 4th Quarter Nitrate 2013 Lab Sample ID: 1310396-005 Client Sample ID: TWN-03_10172013 Collection Date: 10/17/2013 0627h Received Date: 10/18/2013 lOOOh Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Chloride mg/L 10/21/2013 195811 E300.0 50.0 163 Nitrate/Nitrite (as N) mg/L 10/22/2013 2107h E353.2 2.00 23.5 Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of the previously issued reports. Qual Report Date: I 0/30/20 13 Page 8 of 20 All ana]y~~ appliL-.lhte to th.: CWA. SOWA. and RCRA are performed in accordance to NELAC protocols Pertinent sampling iofonna1ion is locatc..J on the at1achcd COC. Confidential Business lnfom.ation: This report is pn1\idci.l fOr the cxclusiv.;! use l>fthc ~ddressee. Pri\·il~cs o!" s~St.~ent ~ oflhc ~c of this .co"?pany or any ~mb1.."T of its staff. or rcpn.xJucti~ ~~this rcpo~ in ~O~cclion~ \\ith the ~~ertiscml-'111. p~omoti~n ~sale of~~}" roo~1 or P~?CI.!SS, ~r in ~-on~~ion W!lh I""; ";-p~blication of this report American West At..IALYTICAI lABORATORIES 463 West 3600 South )alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 4th Quarter Nitrate 2013 Lab Sample ID: 1310396-003 Client Sample ID: TWN-04_10162013 Collection Date: 10/16/2013 0814h Received Date: 10/18/2013 1 OOOh Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Chloride mg!L 10/21/2013 162911 E300.0 5.00 29.4 Nitrate/Nitrite (as N) mg!L 10/22/2013 2104h E353.2 0.500 1.69 Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of the previously issued reports. Qual Report Date: 10/30/2013 Page 6 of20 All analyses applicable lo lhc CWA. SDWA. and RCRA :ul! performed in accortlance lo NELAC prolocols. Pcrtinenl sampling infonnalion is located on lhe atlachctl COC Confillcnlial Business Jnfonnation: This R1JOrt is pro\ided tOr the exclusive use ofthe ~ddrcsscc PrivJlc~cs o! su~~cnt ~of the ~arne of this~con:pany or any ~~bt.'T of i1s s1afT, or rcpmductlo!!. ~fthis rcpor; in ~on~cction ... with the a~vcrtiscmcnt. p~~lio.n or sale of ~~y ~rod~t or p~css, ~r in ~on~c~ion w!th th: r:-publica1ion of Lhis n·por1 463 West 3600 South ;a!t Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 4th Quarter Nitrate 2013 Lab Sample ID: 1310396-001 Client Sample ID: TWN-07 _1 0162013 Collection Date: 10/16/2013 0625h Received Date: 1 0118/20 13 1 OOOh Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Chloride mg!L 10/21/2013 1543h E300.0 1.00 5.70 Nitrate/Nitrite (as N) mg!L 10/22/2013 2042h E353.2 0.100 0.986 Reissue of a previously generated report. Information has been added, updated. or revised. Information herein supersedes that of the previously issued reports. Qual Report Date: I 0/30/2013 Page 4 of 20 All analyses applicable lo the CWA. SDWA, and RCRA are performed in accortlance to NELAC prolocols. Pcrlin.enl ~mpling information i.o; located on the attached COC. Confidential Business Information: This n:port is prmidcd for the exclusive usc of the ~rcsscc. Pri\·ilc~es o~ subr~'Tit ~of the ~c of this .con:'pany or any ~~er of its staff. or reproduct~ ~~this r~ in ~~ionr \\lth lhc ~vcr1io;e~nt, ~omoli~ or sale of ~~Y. ~rod~t or ~occss, ~r in ~o~c~ion w~th l~ r:_~blicalion of lhis n:port INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Nitrate 2013 Lab Sample ID: 1310396-009 Client Sample ID: TWN-07R_l0152013 Arar vrrcAt 1 AaoRAroRIEs Collection Date: 10115/2013 0724h Received Date: Analytical Results 463 West 3600 South Compound )alt Lake City, UT 84115 Chloride 1 0118/2 0 13 1 OOOh Units mg!L Date Prepared Nitrate/Nitrite (as N) mg/L Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 ~-mail : awal@awal-Jabs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Date Analyzed 10/21/2013 2328h I 0/22/20 13 2057h Contact: Garrin Palmer Method Used E300.0 £353.2 Reporting Limit 1.00 0.100 Analytical Result < 1.00 < 0.100 Qual Report Date: 10/29/2013 Page 12 of20 All anaf)'!-CS applicable tu the-C\\'A, SOWA. and RCRA an; JX'rf\.UlTK'd in accordance lo NELAC rrotocols. Pcr1im:nt ~ling infmmalion is located oolhc atlachct.l COC. Conlidcnlial Busim.'S.." lnfoml3tirnr This report is prO\i<k.'i.l for lhc c~clusi,·t! ltSC of the ~kln."SS~.-c. Pri' ib.:~C!" o~~ub_:-"CQ~nt ~~oft he~~~ oflhis _con~r,.my urany "2.~mbl.!r of its s:t;.lfl orn..,..roducti~ ~~this n~ in~o~.:clion~ \\;lh the ac._!_~crti.<:en_'k!nl. r~onlQtio_n l~r ~lc of~~Y. ~rodt~ct or p~css, ~rin ~-un"';_'C~ion w~t.h t~ n:_-public~tWn oflhi!i n:port INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Nitrate 2013 Lab Sample ID: 1310396-004 Client Sample ID: TWN-18_10162013 ANA LY TI CA L LAooRATORIEs Collection Date: 10116/2013 0858h Received Date: Analytical Results 463 West 3600 South Compound )alt Lake City, UT 84115 Chloride 10/18/2013 lOOOh Units Date Prepared Nitrate/Nitrite (as N) mg/L mg/L Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Jabs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Date Analyzed 10/21/2013 1935h 10/22/2013 2106h Contact: Garrin Palmer Method Used E300.0 E353.2 Reporting Limit 10.0 0.500 Analytical Result 67.3 2.15 Qual Report Date: 10/29/2013 Page 7 of20 All anal)'scs applicable tu the CWA. SDWA. and RCRA are performt.-d in acron.Jancc to NELAC protocols. Pertinent sampling infonnation i/'i located on I he attached CDC Confidential Busim.-ss Jnformaliun: This report is prU\;ded for the cxclmi\·c usc of the ~i.ldrcsscc PJi\·iJc~~ or Slll?'=q~"Trt ~of the~ ofth\s ,c~paO)' or any ~~bl'T Of its staff. or reproduc.tio~ ~~I his I'L'fK>~ in ~O~tction~ \\ith the ~\'ertlscmcnl. ('l~omo1io.n OJ s.aJc ofa~y ~rod~1 OT p~ocess, ~r in ~on~! ion W~lh I~ ":-publication or this rt:p011 463 West 3600 South )alt Lake City, UT 84115 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (801)263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Chloroform 2013 Lab Sample ID: 1310621-008 Client Sample ID: TW4-22_10292013 Collection Date: 10/29/2013 1227h Received Date: 10/31/2013 0935h Analytical Results Date Compound Units Prepared Chloride mgiL Nitrate/Nitrite (as N) mg/L Date Analyzed ll/3/2013 0936h ll/512013 2049h Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual E300.0 100 501 E353.2 10.0 45.2 Report Date: II /7/20 13 Page 13 of 34 All ann lyses opplirohlr: lu Jhc CWA, SDWA. <tnd RCRA :m: pcrfolfllC'tl in accordmce lo NElAC protocols. Pertinent sampling infOJl'Jlalion is )I)(;Olted on !he attached CDC. Cunfilkntial Business lnformaliun: This report is pmvi&d for tlu: exclusive usc ofthe ~ddrcs..~·c. Pri~·ilc~~ o!'sub;-.c~n1 ~~of the~ ufthis._co1~pany or any ~~1>\.'7 of ils stdf. or rcproducti~ ~fthis TL"JK>l! in ~'tlion~ \\ilh the ~\'cl1iscmcn1, p~omolio_n or sak: uf ?~Y ~~cl OJ p~~· ~r in ~o~~ion w~th t~ n;.·publit::.rion of this repon American West ANALY TICAL LABOFlATORIES 463 West 3600 South :lalt Lake City, UT 84115 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (801)263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Chloroform 2013 Lab Sample ID: 1310621-003 Client Sample ID: TW4-24_10292013 Collection Date: 10/29/2013 1220h Received Date: 10/3112013 0935h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 1113/2013 0740h 1115/2013 2035h Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual £300.0 100 1,030 £353.2 10.0 34.6 Report Date: lln/2013 Page 8 of34 AU nroly.se.."' applicabl~;: 10 the CWA. SDWA, ant.! RCRA arc pcrfol11'ie1J in accordance lo NELAC protocols. Pcrtin~nt sampling informalioo is located on t~ atlachC'd COC. Cllnfkkntial Buslncs:s lnfonn::.tion: Thi., rqKtl1 i!.; pnwidcJ for~ c.'d~r.·c usc ofthe ~ddn:s~-c. J>ri\;lc~cs o: ~ub~scq~'"Tlt ~c of I he ~~c oflhis .'on?("Qny or ;:my ~"mlx.'T of its staff. or rcproduc1io~ ~f this rcpo~ in ~on?'-'ctiol~ ~ilh lhc ~vcrti..-.c~"lll. ~rio_n ~ ~lc of~~ ~uct t.M' ~~"'!>, ~r in ~"'~~ion w~th t~ r:·p~hlication ofthi~ l\T'Of1 American West AN~t VTl CA l LAeOAATORifS 463 West 3600 South )alt Lake City, UT 84115 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Chloroform 2013 Lab Sample ID: 1310621-002 Client Sample ID: TW4-25_10292013 Collection Date: 10/29/2013 1204h Received Date: I 0/31/2013 093 5h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed I 1/3/2013 0716h ll/5/2013 2033h Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual E300.0 50.0 88.6 E353.2 1.00 6.10 Report Date: lln/2013 Page 7 of34 All un.1lysc.s npplic<:~hle to1he CWA. SOWA. and RCRA arc pcrformctl in accnn:bnce to NELAC prolo.;oh Pt!rtinent :'iampting infomtr.liun i.." loc~ted on the attached COC. Confidrnti31 Burincs.~ ln"fom'llrion: Thi~ rep.•n is pru\itkd for the culus"iw U!>C oftht: ~tldn::s..<>cc. Pri\·ilc~c." o~ sub;-c~cn1 ~c of the ~~~lC of this .con,tpany or any~~ of it-; staff. or n:producti~ ~~this rcpo~ in :on~ction~ v.ilh lhc ~crtio;c~nl, ~o:nlOri~ ~~It: of~~~~ or ~'CSS, ~r in ~o~!ioo w~tb I~ ":_~hliCilrion "fthi.o; n:porl 463 West 3600 South )alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 ~-mail: awal@awal-labs.corn web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Chloroform 2013 Lab Sample ID: 1311306-014 Client Sample ID: TW4-60_11142013 Collection Date: 11/14/2013 0700h Received Date: 11115/2013 0850h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 11122/2013 1232h 11/15/2013 1735h Contact: Garrin Palmer Method Reporting Analytical Used Limit Result Qual E300.0 1.00 < 1.00 E353.2 0.100 <0.100 Report Date: II /26/2013 Page 19 of 45 All analyses opplicuble to the CWA. SDWA, and RCRA ::JJ"\! perfom1etl in accordance to N6LAC protocols Pcr1inent sampling infom~ution is located on the atlached COC~ Confidential Business lnfonnation: This report is provided fort he e)(clusivc usc of the ndtlrcssccJ Privileges of subsequent usc of the name of this com puny or any me~1hcr of its slafr. or rcprod.uctio~ ~this rcpo~ in ~nn~1.:ction~ with the a~vcrtiscmcnt, p~omotio,n o.r ~ale of~~Y. ~rod~ct or p~occsti, ~r in :onm~c!ion w!1h th7 r~-p~blication or this n:por: INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Nitrate 2013 Lab Sample ID: 13I 0396-008 Client Sample ID: TWN-60_IOI72013 ANALYTICAL LABORATORIEs Collection Date: IO/I7/20I3 0845h Received Date: Analytical Results 463 West 3600 South Compound :>alt Lake City, UT 84II5 Chloride I 0118/2013 I OOOh Units Date Prepared Nitrate/Nitrite (as N) mg/L mg/L Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 ~-mail: awal@awal-labs.com web : www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Date Analyzed 10/21/2013 2108h I 0/22/2013 2052h Contact: Garrin Palmer Method Used E300.0 E353.2 Reporting Limit 1.00 0.100 Analytical Result Qual < 1.00 < 0.100 Report Date: 10/29/2013 Page II of20 All anai)'SC.S applic-.lblc lo lhc CWA, SDWA. and Rl'RA arc ('IC"rfmTnt.'tl in accordallt'C 10 NELAC ['Niocols, P~rtinc-nl sampling infonnation is ICK.:Ilh .. "l... on the auachctl COC. Confiikntlal Busincs.o; lnfom\alion: This n:port is pro\·itkd l(lr th~: exclusiYi: usc of the ~n."SSL'C Pri\·ilc~cs o~sub;"C\{~II.mt ~ oflhc ~:u_nc orthis.con~pany or any ~dx.'fofits .staff, or rcproductirn~ ?,fthis n:pm~ in ~n~-clilm~ \\ilh lhc ~\'crtiscnlenl. ~tio.n ~~lc of~~Y .. ~rod~ I or p~ess, ~r in :'On'":-c!ion w!lh t~ ':p~blic<~lion oflhi.-. n:port INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 4th Quarter Nitrate 2013 Lab Sample ID: 1310396-007 Client Sample ID: TWN-65_10162013 ~NAtvrl c At l AaoRATORirs Collection Date: 10116/2013 0727h Received Date: Analytical Results 463 West 3600 South Compound ~alt Lake City, UT 84115 Chloride 10/18/2013 1 OOOh Units Date Prepared Nitrate/Nitrite (as N) mg/L mg/L Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Date Analyzed 10/21/2013 2045h 10/22/2013 2050h Contact: Garrin Palmer Method Used E300.0 E353.2 Reporting Limit 5.00 0.100 Analytical Result 27.1 1.48 Qual Report Date: I 0/29/20 13 Page I 0 of 20 All analyses urrli..Olblc to lhc CWA. SDWA. and RCR...\ are rcrfonm'd in accurdancc to NELAC protocols Pertinent :sampling infonnaiJOn is Jocakd on I he <tltachC'1.1 CDC. Confilk:ntiol Business lnfomlatilm: This. n:port is pruvilktl for the I!Xclusi'\C u..._-.c of the ~li..Jrcs~"'C-Pri\;k~~ or~ub .... Soeq~'f\1 ~or the ~~-m: of lhis .. con!p:lny or lliiY ~-mb-..T of its .slafT. or rcproducti~ ~~this n'fll)~ in ~on~ction~ with the B~\'cl1iscmcnt. P~''o:n l~ ~lc or ~~Y. J?"oth.~·· or (l~"'-~. ~r in ~'On~~ion w~th ·~ r:-rublicalion of lhi~ T\.1l0rt American West Jl l Al¥HQ.AI l"IIOIIAfr.>ll lll! 463 West 3600 South ;ait Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Garrin Palmer Energy Fuels Resources, Inc. 6425 S. Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: 4th Quarter Nitrate 2013 Dear Garrin Palmer: LabSetiD: 1310396 American West Analytical Laboratories received 12 sample(s) on 10/18/2013 for the analyses presented in the following report. American West Analytical Laboratories (AWAL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. This is a revision to a report originally issued 10/29/2013. Some Client Sample ID's have been updated. Pages 1, 2, 4, 5, 6, 8, and 9 have been revised. Thank. You, Approved by: Ky I e F . Digitally signed by Kyle F. Gross DN: cn=Kyle F. Gross, o=AWAL, ou=AWAL-Laboratory Director, G roSS email=kyle@awal-labs.com, c=US Dale: 2013.10.30 13:34:26 -{)6'00' Laboratory Director or designee Report Date: 10/30/2013 Page I of20 All anai)'5C.s applicable to the C\\'A, SDWA. and RCRA arc performed in accordance to NELAC protocols. Pertinent sampl-Ing information i.s located on the a Hac hell COC Confitkntial Busincs...;; Information: This repor1 is pro\ idcd for the exclusive usc of the ~tldrcssce. Pri\ ilc~cs o: sub_scq~cnt ~ oflhe ~~~e uf this 1con!pany or any ~'>Jllbcr of its staff. or rcproducliu.!! of this rcpo~ in ,con~cction. \\-ith the a~yertiscmcnt, p!omolio1n or sale of ?~Y ~rod~cf or p~occss, ~r in ~on~c~ion w~th th~ r:_-publicalion of !hi., report SAMPLE SUMMARY American West Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer ANALYTICAL LABORATORIES Project: 4th Quarter Nitrate 2013 Lab Set ID: 1310396 Date Received: 10/18/2013 1 OOOh Lab Sample ID Client Sample ID Date Collected Matrix Analysis 463 West 3600 South 1310396-00 1A TWN-07 10162013 10/16/2013 0625h Aqueous Anions, E300.0 ~alt Lake City, UT 84115 1310396-0018 TWN-07 _10 162013 10/16/2013 0625h Aqueous Nitrite/Nitrate (as N), E353.2 131 03 96-002A TWN-01_10162013 10/16/2013 0727h Aqueous Anions, E300.0 1310396-0028 TWN-01 10162013 10/16/2013 0727h Aqueous Nitrite/Nitrate (as N), E353.2 Phone: (801) 263-8686 1310396-003A TWN-04 10162013 10/16/2013 0814h Aqueous Anions, E300.0 Toll Free: (888) 263-8686 1310396-0038 TWN-04 10162013 10/16/2013 0814h Aqueous Nitrite/Nitrate (as N), E353.2 Fax: (801) 263-8687 1310396-004A TWN-18_10162013 10/16/2013 0858h Aqueous Anions, E300.0 1310396-0048 TWN-18 10162013 10/16/2013 0858h Aqueous Nitrite/Nitrate (as N), E353.2 ~-mail: awal@awal-labs.com 1310396-005A TWN-03 10172013 10/17/2013 0627h Aqueous Anions, E300.0 1310396-0058 TWN-03 10172013 10/17/2013 0627h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 1310396-006A TWN-02_10162013 10/16/2013 0950h Aqueous Anions, E300.0 1310396-0068 TWN-02 10162013 10/16/2013 0950h Aqueous Nitrite/Nitrate (as N), E353.2 1310396-007A TWN-65 _10162013 10/16/2013 0727h Aqueous Anions, E300.0 Kyle F. Gross 1310396-0078 TWN-65_10162013 10/16/2013 0727h Aqueous Nitrite/Nitrate (as N), E353.2 Laboratory Director 1310396-00SA TWN-60_10172013 10/17/2013 0845h Aqueous Anions, E300.0 1310396-0088 TWN-60 10172013 10/17/2013 0845h Aqueous Nitrite/Nitrate (as N), E353.2 Jose Rocha 1310396-009A TWN-07R 10152013 10/15/2013 0724h Aqueous Anions, E300.0 QA Officer 1310396-0098 TWN-07R_10152013 10/15/2013 0724h Aqueous Nitrite/Nitrate (as N), E353.2 1310396-010A Piez-01_10162013 10/16/2013 l105h Aqueous Anions, E300.0 1310396-0108 Piez-0 1 10162013 10/16/2013 1105h Aqueous Nitrite/Nitrate (as N), E353.2 1310396-0llA Piez-02 101620 13 10/16/2013 1010h Aqueous Anions, E300.0 1310396-0118 Piez-02_10162013 10/16/2013 1010h Aqueous Nitrite/Nitrate (as N), E353.2 1310396-012A Piez-03 _10162013 10/16/2013 1035h Aqueous Anions, E300.0 1310396-0128 Piez-03_10162013 10/16/2013 1035h Aqueous Nitrite/Nitrate (as N), E353.2 Reissue of a previously generated report. Information has been added, updated, or revised. Information herein supersedes that of the previously issued reports. Report Date: I 0/30/2013 Page 2 of20 All analyses applicable lo the CW A. SDWA, and RCRA nrc pcrfOTTTlCd in accordance to NElAC protocols. Pertinent sampling lnfonna1ion is localcd on the attached COC Confidential Buslncss Information: fhjs report is prm;dcd for Lhc cxclusi\·c usc of the ~lldrcsscc. Prl\·ilc~cs 0~ sub~scq~cnt ~oft he ~~~cor this ... co~pany or any "!;'lllbcr of its staff, or rcproducli~ ~fthis rcpo~ In ~on~cction~ Y.ith the ~vcrtisc~nt, ~omolio.n or sale oF ~~y rnld~cl ur p~ocess, ~r in :onn:_c~ion W~lh n .. : rc-publicalion of Ibis n!port 463 West 3600 South ;alt Lake City, UT 84115 Phone: (801) 263-8686 foil Free: (888) 263-8686 Fax:(801)263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Garrin Palmer Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: 4th Quarter Nitrate 2013 1310396 10/18/2013 10115, 10/16 & 10117/2013 Intact None Holding Time and Preservation Requirements: The analysis and preparation for the samples were performed within the method holding times. The samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, DUP: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Duplicate (DUP): The parameters that required a duplicate analysis had RPDs within the control limits. Corrective Action: None required. Report Date: I 0/29/2013 Page 3 of 20 All analyses applirohle h.) the CWA. SD\\' A. and RCRA arc rcrformed in accordance to NELAC pro1ocols Pertinent sampling information is located on the attached CDC Confit.k:ntial Business Jnfonnation: This n!port is pnwjdcd for the C;\c)~Yc usc oflhc ':ddrcs.sce Pri\·il!:~cs o~ suh!cq~cnt ~o;e of the ~:u_nc ofthls .con~p:~ny or any "_!'lTlbL'T of irs staff. or rcprodue1i~ ~~this rcvo~ in ~on~cction~ wi1h the ~~cJ1iser1_1cnl. p~omolio.n or sale of~~ ~rod~1 or pr_occs..", ~r in :onncc~ion \\ !'h I~ rc~publication of this report American West ANALYTICAL LABORATORIES 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 1310396 Project: 4th Quarter Nitrate 2013 Analyte Lab Sample ID: 1310396-006BDUP Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) Lab Sample ID: 1310396-0llBDUP Test Code: N02/N03-W-353.2 Nitrate/Nitrite (U5 N) Result Units Method Date Analyzed: l 0/25/2013 l856h 113 mg/L E353.2 Date Analyzed: 10/25/2013 185911 0.374 mg!L E353.2 MDL 0.252 0.00252 Reporting Limit 10.0 0.100 Dept: we QC Type: DUP Amount Spiked Spike Ref. Amount %REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt •1. RPD Limit Qual 119 4.73 20 0.371 0.671 20 Report Date: I 0/29/20 13 Page 16 of 20 anRlyscs upplicablc to the CWA. SDWA,und RCRA urc pcrfollncc.J in Hccorc.lancc to NELAC f!rotocols. Pertinent sampling infonnatjon is locutcd on the attached COC. Conlidcntinl Business lnfom1a1ion: This report is provided for the exclusive usc of the addressee. Privilcgi.'S of subsequent usc oft~ UC' of this company or any member of ils ~tufl Ol' rcprodllction of this 1cport in connection with tht: udvcrtiscmcnt, promotion or sale of any product or process. or in connection with the rc~publicution of I his report for any purpose oth~.·r than for the uddn:sscc will be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1310396 Project: 4th Quarter Nitrate 2013 Analyte Result Lab Sample 10: LCS-R60535 Date Analyzed: Test Code: 300.0-W Chloride 4.79 Lab Sample ID: LCS-R60574 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.01 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Garrin Palmer Dept: we Units Method MDL I 0/21/2013 141 Oh mg/L E300.0 0.0114 I 0/22/2013 2041 h mg/L E353.2 0.00252 Reporting Limit 0.100 0.100 QC Type: LCS Amount Spiked 5.000 1.000 Spike Ref. Amount 0 0 o/oREC 95.8 101 Limits 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt % RPD Limit Qual Report Date: 10/29/2013 Page 17 of20 I analyses upplicablc to the CWA. SDWA, und RCRA urc pcrfonncd in uccortlancc to NELAC protocols~ Pertinent sampling infonnation is located on the attached COC. Confidential Business lnfonnation: This report is provided for the exclusive usc of the addressee. Privileges of subs~,..-qucnt usc of tt nc of this company or any member of its staff, m· reproduction of this report in connection with I he advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the uddrcsscc will be granted only on contact. This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1310396 Project: 4th Quarter Nitrate 2013 Analyte Result Lab Sample JD: MB-R60S3S Date Analyzed: Test Code: 300.0-W Chloride <0.100 Lab Sample ID: MB-R60S74 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) <0.100 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (80 I) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC_SUMl\'IARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 10/2112013 1347h mg!L E300.0 0.0114 0.100 I 0/22/2013 2039h mg/L E353.2 0.00252 0.100 Garrin Palmer we MBLK Spike Ref. Amount e;.REC Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt e;.RPD Limit Qual Report Date: I 0/29/20 13 Page 18 of 20 1 tlnalyscs upp\icablc to the C:WA. SDWA, und RCRA urc performed in nccorcluncl.' ro NELAC protocols. Pertinent sun1pling infonnation is loci.\ ted on the attached COC, Confid~:nti;ll Business Information: This report is pn.widcd for the exclusive usc oft he addl'\:"SSC<.',. Privileges of subsequent usc of tJ. nc of this company or uny member of its stntT. Ol' n:produ~.:tion of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the rc-pubiication of this report for any purpo~c other than for the tu..ldn:sscc will be gmntcd only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1310396 Project: 4th Quarter Nitrate 2013 Analyte Result Lab Sample ID: 131 0396-00SAMS Date Analyzed: Test Code: 300.0-W Chloride 4.97 Lab Sample ID: 1310396-011 BMS Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.33 Units 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com QC SUMMARY REPORT Contact: Garrin Palmer Dept: we Method MDL Reporting Limit QC Type: MS Amount Spiked Spike Ref. Amount %REC 10/21/2013 2131h mg/L E300.0 0.0114 0.100 5.000 0 99.3 10/22/2013 2110h mg/L E353.2 0.00252 0.100 1.000 0.364 96.3 Limits 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt '"!. RPD Limit Qual Report Date: 10/29/2013 Page 19 of20 I analyses upplicablc to the CWA. SDWA. and RCRA urc pcrfonncd in uccorduncc to NELAC protocols, Pertinent sump ling information is located on the attached COC Clmfidcntial Business lnfom>alion: This report is provided for the exclusive usc oft he addressee, Privileges of subsequent usc oftt 11c of this company or any member of its stun: or rcprmJm:tion of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the-rc·publication of this report for uny purpose other than for the addn:sscc will be grunted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1310396 Project: 4th Quarter Nitrate 2013 Analyte Result Lab Sample ID: 1310396-00SAMSD Date Analyzed: Test Code: 300.0-W Chloride 5.00 Lab Sample ID: 1310396-0liBMSD Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.41 463 West 3600 South Salt Lake City, UT 84115 Phone: (801 ) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Garrin Palmer Units Method 10/2112013 2155h mg/L E300.0 10/22/2013 2115h mg!L E353.2 MDL O.QII4 0.00252 Reporting Limit 0.100 0.100 Dept: we QCType: MSD Amount Spiked 5.000 1.000 Spike Ref. Amount 0 0.364 %REC 100 104 Limits 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual 4.97 0.762 20 1.33 5.76 10 Report Date: 10129/2013 Page 20 of20 1 una lyses applicable to the CWA, SDWA. and RCRA urc pcrform~d jn accortluncc to NELAC protocols~ Pcrtincnt sampling information is located on the attached COC, Confidential Business Information: This report is provided for th1..· exclusive usc or the addressee. Privileges. of s.ub~cqucnt usc Qf t~ nc of this company or any mt:mbcr of its stutl: ot· rcproductlon of this report in connection with the advertisement. promotion or sak· of any product or process. or in connection with the-rc~publkution of this report for any purpose other than for the adllrcssr.:-c will be gro:~.ntcd only on contact This UL American West Analytical Laboratories REVISED: 10-30-13 Denison Sample ID's updated -RW WORK ORDER Summary Work Order: 1310396 Page 1 of2 Client: Energy Fuels Resources, Inc. Due Date: 10/29/2013 Client ID: DENlOO Contact: Garrin Palmer Project: 4th Quarter Nitrate 2013 QC Level: III WO Type: Project Comments: PA Rush. QC 3 (Summary/No chromatograms). MUST report project specific DL's: Cl@ 1 mg/L, N02/N03@ 0.1 mg/L. EDD-Denison & LOCUS. Email Group; Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1310396-001A TWN-07_10162013 1 0/16/2013 0625h 10118/2013 1000h 300.0-W Aqueous l\/ df-cl --- - I SEL :'_ii!(IJ.r.t_£1!_: CL 1310396-0018 N02/N03-W -353.2 ~ df-no2/no3 I SEL Analytes: N03N01N 131 0396-002A TWN-01_10162013 10/16/2013 0727h 10/18/2013 IOOOh 300.0-W Aqueous v df-cl 1 SEL Analytes: CL 1310396-0028 N02/N03-W-353.2 ..t' df-no2/no3 1 SEL Ana{vtes: N03N01N 1310396-003A TWN-04_10162013 10/16/2013 0814h 10/18/2013 IOOOh 300.0-W Aqueous ~; df-cl 1 SEL Analytes: CL 1310396-0038 N02/N03-W-353.2 loll df-no2/no3 1 SEL Ana{vtes: N03N01N 131 0396-004A TWN-18_10162013 10/16/2013 0858h 10/18/2013 IOOOh 300.0-W Aqueous 1'{1 df-cl 1 SEL Analytes: CL 1310396-0048 N02/N03-W-353.2 .-f. df-no2/no3 1 SEL Ana(vtes: N03N01N 131 0396-00SA TWN-03_10172013 10/17/2013 0627h I 0/18/20 13 I OOOh 300.0-W Aqueous ~l df-d I SEL Ana(vtes: CL 1310396-0058 N02/N03-W-353.2 ~ df-no2/no3 I SEL Ana(ytes: N03N01N 131 0396-006A TWN-02_10162013 I 0/16/2013 0950h 10/18/2013 1000h 300.0-W Aqueous ~ df-cl I SEL Analytes: CL 1310396-0068 N02/N03-W-353.2 "'' df-no2/no3 1 SEL Analytes: N03N01N 1310396-007A TWN-65_10162013 10/16/2013 0727h 10/18/2013 IOOOh 300.0-W Aqueous ~ df-cl I SEL Analytes: CL 1310396-0078 N02/N03-W-353.2 ~] df-no21no3 I SEL Analytes: N03N01N 1310396-008A TWN-60_10172013 10/17/2013 0845h 10/18/2013 IOOOh 300.0-W Aqueous ~ df-cl I SEL Analytes: CL Printed: I 0/30/20 I 3 WORK ORDER Summary WorkOrder: 1310396 Page 2 of2 Client: Energy Fuels Resources, Inc. Due Date: 10/29/2013 SampleiD Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 131 03 96-008B TWN-60_10172013 10/17/2013 0845h 10/18/2013 1000h N02/N03-W-353.2 Aqueous ~ df-no2/no3 1 SEL Ana(vtes: N03N02N 1310396-009A TWN-07R_101520l3 10/15/2013 0724h 10/18/2013 1000h 300.0-W Aqueous ~ df-cl I SEL Ana(vtes: CL -- -----1310396-0098 N02/N03-W-353.2 .. .j' df-no2/no3 I SEL Ana(vtes: N03N02N 1310396-010A Plez-01_10162013 10/16/2013 I JOSh 10/18/2013 IOOOh 300.0-W Aqueous ~ df-cl --I S~L Analytes: CL ~- 1310396-0108 N02/N03-W-353.2 ~ df-oo2/no3 I SEL Analytes: N03N02N 1310396-011A Piez-02 _1 0162013 I 0/16/2013 I 01 Oh 10/18/2013 IOOOh 300.0-W Aqueous >/ df-cl 1 SEL Analytes: CL 1310396-0118 N02/N03-W-353.2 ~ df-no2/no3 I SEL Ana{vtes: N03N02N 131 0396-012A Plez-03_10162013 10/16/2013 1035h 10/18/2013 1000h 300.0-W Aqueous r-1 df-cl 1 SEL Analytes: CL 1310396-0128 N02/N03-W-353.2 ~ df-no2/no3 I SEL Anaf.vtes: N03N02N Printed: I 0/3012013 3 ; 4 American West Analytical Laboratories L~ 48S W. 3600 S. SanLak9 City, UT 841 1 5 Phone II (801)263-eee& Toll Freet (888)2flS.a686 Fal t (801)263-8887 Email aweiOa'Mll-labB.com www.awal·labs.com Client: lllllellD' Fa.ela Reaourcu, ID.c. Addl1181: 84215 B. Hwy. 191 BlandiDf, UT 84811 Contact: GurlD Palmer Phone I: (4315) 878·2221 Cell f : ~~ok.CIO:m; ICWi:daol.•eo.o:rcyfllU:C~ Email: 4tu!!I!!""'S11115bl.com Project Name: 4tb Quarter Nitrate 2013 Pro)ecU: POt: sampler Name: Gurlll Palmer, TlmD.er Holliday ·SamtlleiD: Date Samoled ~7_1ou12013 * TWN-07 10162013 10(16/2013 TWN-~2013 * TWN-01 10162013 10/16/2013 TWN"""'-1.018~ * TWN-04 10162013 10/18/2013 TWN·18_10162013 10/18/2013 Tw.N-s_1~ * TWN-03 10162013 10/17/2013 ~2...101621)13 * TWN-02_10162013 10/18/2013 TWN-811_10182013 10/18/2013 TWN-80_10172013 10/17/2013 1'WN-G7R..1011SI013 10/15/2013 Pl..Ol_lOUII013 10/18/2013 Plea-Q1_10le2013 10/18/2013 Pleii...03_10181013 10(18/2013 'l;emp Bluak ROIInqulll\0<1 til': s~gna~w (, '~~ ~(t?ll'.! P~ni.Nomo.· O~r+--'""' f c...l .,.....,-lt.~O f'IOiinqulll\0<1 by: ~~ PtW ~"' ROIInqU10110dtl\': SIOnaturo ~NNa!ne: ROitnqv-t>y: Slgnal\n iPrf!ll~ CHAIN OF CUSTODY AI ~will t.oonductod~ NEI.AP -odiTlllltclds...Soll-lllllt. -"'<i~AWAL'a-..w,te RQ-..1~ llmils(f'OI.) ....... ..,...alcaly.....-al-oollllsCholnd!:uSody __ _ QC Level: Tum Around Tme: ~"~!lor---""""..-. ~~wlbo...-bJ5:00pmoo 3 Standald ... ..,..., __ X lnclud& EDO: LOCUS UPLOAD UCIIL Field Fllaled For. For~Wftll: 0 NE!.AP 0 RCRA 0 CWA 0 SOWA 0 ELAP/#1..2LA 6' 0 NLLAP ~ 0 0 Non-Compliance ~ 0 D Olher. <') ; ~ Is ~ <>l i 0 8 :::E !!:. ll) Known Hazards nme 8 l N ~ & Samoled 0 i a Sample Comments .... 62lS 3 w X X 771 :z w X X 81. 2 ., X X 8S8 2 w X X 637 2 ., X X 950 2 \V X X 771 2 w X X MIS 2 w X X 714. 3 w X X nos 2 w X X 1010 2 w X X 10311 3 w X X l w :=:.by.· ~ .. ~ Instructions: !)/() 51G, #I..WN..l.ab ~Salt Page I ol ru·~~ ~Use~ty' ~w-R:o{-)\ :0.8 s "----:.t.:!:L. 'C ··---~ ~0 y • &a:-V . 'N ·-· .., N •-w-(!j~ N COC;~•W• k Hoi, <::>CliO..~ 2~00 Olijo l'!dlOQO N W. ~ "'-'"'~ e y N 4~ ... ~@ ·y N ~-~ y k l.loblils-rodc;oc~ " nme: *Sample ID's updated, per Kathy Weinel Pdo!NIIIM:. ~k d.l ......,. !~'//?-/& 10/30/13 -RW Pm:~UY\~ ~l "..J ITmo.' l'HJo =tii'J { ~ jTime: !'rlni Norno: ~"'tlf. 0.: 'SlO'IIII\ft nme: PriniNome! I Analysis Ammonia COD Cyanide Metals NOz&N03 O&G Phenols Sulfide TKN TP04 Procedure: Frequency: Preservation Check Sheet s ,le Set E Preservative I :t.. a t/ J (o pH<2 H2S04 oH<2 H2S04 pH>12 NaOH pH<2HN03 oH<2 HzS04 .j,.-s v.es J'e-.~ ./~ !l'cl ~J pH<2HCL 17 II 1/ 11 I' oH <2 H2S04 pH>9NaOH, Zn Acetate pH <2 H2S04 pH <2 H2S04 - - Pour a small amount of sample in the sample lid Pour sample from Lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid 7 tt.r I doH I? 9 Jfs-y,;. ~ /cl II y~ d~/ 7 - 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * The sample required additional preservative upon receipt. + The sample was received unpreserved • The Sample was received unpreserved and therefore preserved upon receipt. # The sample pH was unadjustable to a pH< 2 due to the sample matrix • The sample pH was unadjustable to a pH> __ due to the sample matrix interference Lab Set ID: /3 lo 3 ~(p /7._ tfq- [7 American West ANAl VJICAL \ AIJO~ATO~IfS 463 West 3600 South )alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Garrin Palmer Energy Fuels Resources, Inc. 6425 S. Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: 4th Quarter Chloroform 2013 Dear Garrin Palmer: Lab Set ID: 1310621 American West Analytical Laboratories received 11 sample( s) on 1 0/31/20 13 for the analyses presented in the following report. American West Analytical Laboratories (AWAL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Approved by: Ky I e F . Digitally signed by Kyle F. Gross DN: cn=Kyle F. Gross. o=AWAL, ou=AWAL·Laboratory Director, G email=kyle@awal-labs com. c=US ross Dale: 2013,11.12 14:25:11-07"00" Laboratory Director or designee Report Date: 11/7/2013 Page I of34 All analyses appli~.Wic tolh~: CW A. SDWA. and RCRA an.· ~rfll~d in ac .. ·ord:Jnce I<' NElA( rrutocob. Pcnincnl ~mplin~ infc;mn~lion l .. local~"-' vn the at1.ad1~ COC Con1i~ntial Busincs!' 11\fonnution: TI1is ~IX'" is prmilkd fUr •he c~c:l~i'\e usc of the ~r~~. Pri\'iii.~C~ v~ ~~~~~m ~~o;c of1hc ~~of !.hi;; .c .. •n.lp.1ny ur any~~~~~"' of it~ !\tufl: (.,. o:pro~uclh.~ ~~1his 1\.'flO~ 1n ;un!)~o-<:lit\0__ \\ith lhc ~\t<'f1i~~)l:n1. Jl~omoti~n ~r sale.: of ~~Y. ~TOd~l vr p~~c~<;, ~r in :on~~~ion w!lh t~ '"':"fl~blic.:.lion uf lhi.;; I'L1>nn SAMPLE SUMMARY American West Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer At-4 A L VTICA L lA9 0RA.TOR lfS Project: 4th Quarter Chloroform 2013 Lab Set ID: 1310621 Date Received: 10/3112013 0935h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 463 West 3600 South 131 0621-001A MW-32_10292013 10/29/2013 1330h Aqueous Anions, E300.0 ;alt Lake City, UT 84115 1310621-00 lB MW-32_10292013 10/29/2013 1330h Aqueous Nitrite/Nitrate (as N), E353.2 1310621-001C MW-32_10292013 10/29/2013 1330h Aqueous VOA by GC/MS Method 8260C/5030C Phone: (80 1) 263-8686 1310621-002A TW4-25_10292013 10/29/2013 1204h Aqueous Anions, E300.0 1310621-0028 TW4-25 10292013 10/29/2013 1204h Aqueous Nitrite/Nitrate (as N), E353.2 Toll Free: (888) 263-8686 1310621-002C TW4-25 10292013 10/29/2013 1204h Aqueous VOA by GC/MS Method Fax: (80 l) 263-8687 8260C/5030C !-mail: awal@awal-labs.com 1310621-003A TW4-24 10292013 10/29/2013 1220h Aqueous Anions, E300.0 1310621-0038 TVV4-24_10292013 10/29/2013 1220h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 1310621-003C TVV4-24 10292013 10/29/2013 1220h Aqueous VOA by GC/MS Method 8260C/5030C 1310621-004A TVV4-04_10292013 10/29/2013 1302h Aqueous Anions, E300.0 Kyle F. Gross 1310621-0048 TVV4-04_10292013 10/29/2013 1302h Aqueous Nitrite/Nitrate (as N), E353.2 1310621-004C TVV4-04 10292013 10/29/2013 1302h Aqueous VOA by GC/MS Method Laboratory Director 8260C/5030C 1310621-00SA MVV-04_10292013 10/29/2013 1255h Aqueous Anions, E300.0 Jose Rocha 1310621-0058 MVV -04 _1 0292013 10/29/2013 1255h Aqueous Nitrite/Nitrate (as N), E353.2 QA Officer 1310621-00SC MVV-04_10292013 10/29/2013 1255h Aqueous VOA by GC/MS Method 8260C/5030C 1310621-006A MW-26_10292013 10/29/2013 1246h Aqueous Anions, E300.0 1310621-0068 MVV-26_10292013 10/29/2013 1246h Aqueous Nitrite/Nitrate (as N), E353.2 1310621-006C MW-26_10292013 10/29/2013 1246h Aqueous VOA by GCIMS Method 8260C/5030C 1310621-007 A TW4-19 10292013 10/29/2013 1410h Aqueous Anions, E300.0 1310621-0078 TVV4-19_10292013 10/29/2013 1410h Aqueous Nitrite/Nitrate (as N), E353.2 1310621-007C TVV4-19_10292013 10/29/2013 1410h Aqueous VOA by GCIMS Method 8260C/5030C 1310621-008A TW4-22 10292013 10/29/2013 1227h Aqueous Anions, E300.0 1310621-0088 TVV4-22_10292013 10/29/2013 1227h Aqueous Nitrite/Nitrate (as N), E353.2 1310621-00SC TVV4-22_10292013 10/29/2013 1227h Aqueous VOA by GCIMS Method 8260C/5030C 1310621-009 A TVV4-20 10292013 10/29/2013 1240h Aqueous Anions, E300.0 1310621-0098 TVV4-20 10292013 10/29/2013 1240h Aqueous Nitrite/Nitrate (as N), E353.2 l310621-009C TVV4-20 10292013 10/29/2013 1240h Aqueous VOA by GCIMS Method 8260C/5030C 1310621-010A TW4-65_10292013 10/29/2013 1330h Aqueous Anions, E300.0 1310621-0108 TVV4-65_10292013 10/29/2013 1330h Aqueous Nitrite/Nitrate (as N), E353.2 Report Date: 11/7/2013 Page2 of34 AIL al\:llysc~ ::~pplic<lblc 10 the CWA. SDWA. :md RCRA ~n; (l('r(,lrmed in accunt:Jncc to NElAC prut,~ub:, f\;-n1ntl\l ·~-·-"i'H inf.lmtati<'n h IU('.t1~t (,Ill lhc atbchN COC. Conti~nfl,d ll$..1:D...-.. lnfo~liun: This I"I!Jlt.'r1 is pwvilkJ ~" d)C"t""t.t.loHo oflhL! ~JX:..~c Pri\·lk~~:S o! suh;"Co.t~cnt ~".: of1hc ~~~11! \lf lhis .con~r~any ur any n!:mh~.-1 of it~ ~taff. or TC'Ilrodu.:t~~ f .. ,~11! t11 ~'~IX1\un~ \\ ith !he a.J_VCf1~~'M,."nl. f'~~lnl01~ Or ~]I! •t ~ffi' trf"""''llo:l 01 p~~I.".">S, ~Tin :()Urk,:~iOn W~th ~ f ~ llaiiUAufllti..io n.=J'kU'\ 463 West 3600 South )alt Lake City, UT 84115 Phone: (801) 263-8686 foil Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail : awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Client: Project: Lab Set ID: Energy Fuels Resources, Inc. 4th Quarter Chloroform 2013 1310621 Date Received: 10/31/2013 0935h Lab ample ID Client Snmple ID 131 0621-01 OC TW 4-65 10292013 1310621-011A Trip Blank Date Collected 10/29/2013 1330h 10/29/2013 Contact: Garrin Palmer Matrix Analysis Aqueous VOA by GC/MS Method 8260C/5030C Aqueous VOA by GC/MS Method 8260C/5030C Report Date: 11/712013 Page 3 of34 All anal~s applicable toth~: CWA. SDWA. and RCRA are pcrf<•rmed in accordaocc to NELAC rrotocol<;. Peninem ~mpling infonnallon i~ lo.:atcd on lhc attlchcd COC. ·~'rti"'-nui fht1i~ Jnrontuliun: Thi~ repon is flii.J\'hle:d tbt ~1;,q\.:t yf1~ ~n..~e Prhile~c:. of suh:o;cq~cnl ~~~ ofthc ~~of this .coH_l(lany or any ~~ber ofiL" stllff. or Tcp~ti~ ~rtbl!' rep~ in ~on~'lo •. -cti•m_ \\i'b the ~~-cni~~l\..111,f"~Ufnotil~ ,.,. .Jk urll~ ~"t.lil~1 or p~'t'SS, ~r in :Onn:"X'~iOf' w.!lb t~ r~1JUrotJM.,~ h 463 West 3600 South )a!t Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative CUent: Contact: Energy Fuels Resources, Inc. Garrin Palmer Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-0-C Discrepancies: 4th Quarter Chloroform 2013 1310621 10/3112013 10/29/2013 Intact None Holding Time and Preservation Requirements: The analysis and preparation for the samples were performed within the method holding times. The samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Corrective Action: None required. Report Date: 1117/2013 Page 4 of34 All analyses i1flplicoblc 10 the CWA. SDWA. and RCRA are pcrfonnetl inaccord:Jncc to NELAC proiNol". PeJ'Iin ... "Tl1 sampling infom.Hlliools loc:Jt<!d on 1~ annchl!d COC Confitknlial Bu~incs.o;o 1nfonnarion: Thi...,.n:JlCin ls provided for the cxdusi\·e ~of the ~tJdi'CS.<:t.'C PJiyjJc~~ ors-ub_:cq~L'llt ~of lhc ~~~~C ~Jfthis •COll.l!)<IDY I}( UOy ~~lhCT ofit'i Staff, Of n.llrodUCiiO~ ~f1hjs Tt.'(K'l~ in ~Oil~Ciion,. With 1hc ~~ crti~OX."fft. r~omotio,n ~T ~~C Of~l!)~ ~TO<h~t Of ~ess, ~fin ~0~1:~i00 W~lh 1~ ~lication Oflbl.o; report 463 West 3600 South ;aJt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Energy Fuels Resources, Inc. Garrin Palmer Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-0-C Discrepancies: Method: Analysis: 4th Quarter Chloroform 2013 1310621 10/3112013 10/29/2013 Intact None SW-846 8260C/5030C Volatile Organic Compounds General Set Comments: Multiple target analytes were observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 1117/2013 Page 5 of34 All ;malyscs applicablt: h> Lhc C\\' A. SDWA. aod RCRA ::~re ~rfunncd ln accord:mc~ to NELAC JlrUlocols P<:rtinrol sampling infOTmiilion i:l.lltea1eJ on 1ht.· 311ltchcd COC Confidcnlial Blhi.ncs.s )nfQml:lti(m: Thi~ n:p.1n ts pnni&d tOr lhe exclusi\'C I..I:!K: of lhe ~Jdrc~c. Pri\ilc~cs o~ sub~scq~--n1 ~....:or the~~ of Lhis .con .. pany or any ~~mbt.'T of il<t s13ff. (lf n:pro.l~li~ ~ftlli<: r.::p.~ 1n ~~cclit:Rl~ \\i1h lhc u..J_vcrti~~l1.111, ~umoliO,O ~ ~lc IJf ~Y. ~od~l \M" ~~~!!$..~Tin :(~~ioo w~th I~ r~-puMica1ion of lhi'i n:por ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 1310621 Project: 4th Quarter Chloroform 2013 Analyte Result Lab Sample ID: LCS-R61122 Date Analyzed: Test Code: 300.0-W Chloride 4.83 -Lab Sample ID: LCS-R61202 Date Analyzed: Test Code: 300.0-W Chloride 4.63 Lab Sample 10: LCS-R61213 Date Analyzed: Test Code: N021N03-W-353.2 Nitrate/Nitrite (as N) 1.02 463 West 3600 South Salt Lake City, UT 84115 Phone: (80 I) 263-8686, Toll Free: (888) 263-8686, Fax: (80 I) 263-8687 e-mail: awal@awal-labs.com, web: ~'l'w.awal-labs.com Q_C SQ_MM_.ARY REJ?.QR.T_ Units Method MDL 11/03/2013 0008h mg!L E300.0 O.oii4 11/05/2013 1038h mg!L E300.0 0.0114 11/05/2013 2030h mg!L E353.2 0.00252 Reporting Limit 0.100 0.100 0.100 Contact: Dept: QC Type: Amount Spiked 5.000 5.000 1.000 Garrin Palmer we LCS Spike Ref. Amount %REC 0 96.7 0 92.6 0 102 Limits 90-110 90-110 90 -110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: lln12013 Page 27 or34 unulys~.-s npplic:Ibk to th..: CWA. SDWA. :.m<.l RCRA U.t\; p~.:rfonn~.-d in tu:cordanct.· 10 NELA(' prohx· .. )Js. Pt..:"11in..:-nt s:.tmpling infonnution is locatl.~ tm th~ "ttuchcd COC' C'tlllfidcncial H\tsincss lnfomuJiion: This rqxwt is provided f\,r th<: l'Xclu~ivc us~.· of1~ :ukln:s...;"•..,:. Privilcg~..-s of !<illbS~:qlu.·nt us .. • llftt nc of this comoanv or unv mcmb..:r of its stuft: ur l\.'Dhlt.lucliun ufthis rcnort in conne-ction with th~: mlv~.:.·ttis...·m~.mt, promotion ot sale of any protlu~o:l or process, or in \.'Onnccuon witlt the tc-publicat\on or this r~.::pmt I~H any pUf\lt.lS~: uth~o·r than fnt th\.: 1.1dJn.:sscc wil1l'1~o· gmntl'd only on ~.:c.mll.h.:l This AN/..LY"' CAl l..AI'\.O RATO~IES Client: Energy Fuels Resources, Inc. Lab Set ID: 1310621 Project: 4th Quarter Chloroform 2013 Analyte Result Lab Sample ID: MB-R6ll22 Date Analyzed: Test Code: 300.0-W Chloride <0.100 Lab Sample ID: MB-R61202 Date Analyzed: Test Code: 300.0-W Chloride <0.100 Lab Sample ID: MB-R612l3 Date Analyzed: Test Code: N02/N03-W-353.2 NitratefNitrite (as N) <0.100 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com. web: www.awal-labs.com Q~ .. _SILMMARX .REP.QRI_ Contact: Garrin Palmer Dept: we QC Type: MBLK Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 11/02/2013 2345h mg/L E300.0 0.0114 0.100 11 /05/2013 1013h mg/L E300.0 0.0114 0.100 11/05/2013 2029h mg/L E353.2 0.00252 0.100 Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt •.r.RPD Limit Qual Report Date: lln/2013 Page 28 of34 anulyS4..-s npplicablc ro the CWA. ~DWA, und RCRA an: IJ'-:rtbnnL'tl in uccon.lwJcc cu NELAC' prult>~.:ols. Pcrtin~nt s:.ampliug infOm1ution is l,>eatcd on 1h~ aua~.:hcd COC'. c~.,ntid~nli:.ll Busith.:ss lnf'i.1m1ation: ·rhis rqwrl is pmvil.kc.J t~r the cxc.:lusin.· USL' ofth..: ~uk.ln.'Ss~..: Privtlcg'-~ "lf:o;ubSL'Qucnt usL~ oftt nc of this l'Ompany or nny mt:mbCI' uf its statl', \1r ~produdiun of this n:port in l'onnc-dion with th~ ut.JvL'rtis~mcnl. promotion or sa h.· of any product tJr pnx.·cs:s. ur in connL'Clion with th~ n."'-pllblkation of this n:pott ti.w lmy Pllrr'k)SC uthcrthan t\Jr the m.IUr..:~sc~o..· will b..: gmntcd. only un conta..;t This Client: Energy Fuels Resources, Inc. Lab Set ID: 1310621 Project: 4th Quarter Chloroform 2013 Analyte Result Lab Sample ID: 1310621-00IAMS Date Analyzed: Test Code: 300.0-W Chloride 270 -Lab Sample lD: 1310621-00IBMS Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 0.966 463 West 3600 South Salt Lake City, UT 84115 Phone: ( 80 I) 263-8686, Toll Free: (888) 263-8686, Fax: (80 I) 263-8687 e-mail: awal@jawal-labs.com, web: www.awal-labs.com __ QC _ _SU_MM_ARY RE~_QRT Contact: Garrin Palmer Units Method 11/03/2013 0630h mg/L E300.0 II /05/20 13 2040h mg/L E353.2 MDL 0.570 0.00252 Reporting Limit 5.00 0.100 Dept: we QC Type: MS Amount Spiked 250.0 1.000 Spike Ref. Amount 35.7 0 %REC 93.5 96.6 Limits 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt % RPD Limit Qual Report Date: 11/7120 13 Page 29 of 34 tlnulys'-"S upplkab)(' to th~ CWA. SDWA, and RCRA ttr"' p~..·rfolnll..-d in w.:cortlan<.:l.:' to NEL.AC pmtoc:o1s. P~rtin'-·nt sum piing infOrmation is f,>ea.tcd on rh~ uttac.:hcd C'OC. (\lnfid~ntial Uusim:s~ rnft.urnation: fhis 1cpon is tmn id~d fm th~..· ~xdusiv..: us ... • ofth~ ac.J:llrcss~~. Privih:g.~.--s 1..lf sufY..;,.,-qucnl us~ or ct liL' ~)f this t mnpany or any m~mb..:r of its si~Ltl or n.!produ~o:l.ion nf this J'(.·port in l:l)nnl'l'tiun with the ad .... crtiSl.'ITtCnl, promotion or sah: ot·;lny produr.:t or pro~;."'L~-s. 01 in connc~..·tion with the n .. --publication lll' this n:po• t ti.w any purfl4J'il.:' oth~.:r th~m f\w th. .. • addr ... ~~~l" will hi..' granh .. ·d only on """mtad Thi~ ANA LYTICAL lABO FIATOR if:S Client: Energy Fuels Resources, Inc. Lab Set ID: 1310621 Project: 4th Quarter Chloroform 2013 Analyte Result -Lab Sample ID: 1310621-00IAMSD Date Analyzed: Test Code: 300.0-W Chloride 281 Lab Sample ID: 1310621-00IBMSD Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 0.971 463 West 3600 South Salt Lake City, UT 84115 Phone: ( 80 I) 263-8686, Toll Free: (888) 263-8686, Fax: (80 I) 263-86R7 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC_SU_M_MARY REfQRT Contact: Garrin Palmer Units Method 11/03/2013 0653h mg/L E300.0 11/05/2013 2041h mg/L E353.2 MDL 0.570 0.00252 Reporting Limit 5.00 0.100 Dept: we QCType: MSD Amount Spiked 250.0 1.000 Spike Ref. Amount 35.7 0 %REC 97.9 97.1 Limits 90-110 90-I 10 Kyle F. Gross Laboratory Director Jose Rocha QA Otliccr RPDRef. RPD Amt % RPD Limit Qual 270 4.00 20 0.966 0.527 10 Report Date: II n120 13 Page 30 of 34 anulys..:s npplicablc to th~o· C'WA. SDWA, nml RCRA ;tl\: p..:rt'ormc"ll in Ui,;'COrtlun..:~.· UJ NELAC' prut()l'OIS PI.:Jtin .. :nt Slllnpling information is lncah.:tl on th'-' atlal"hl·d coc. (\\lllitkntiul Bu~dm.:ss Information: ('his 1'1.:\l\Jil is Pl\l\ id~tl t~lr the l:'XI..'h&Si\1..' ll~\.· or the tuJllr~SS\.'C. Pri\'ilt:g~:~ or SllbSt:qucnt liS\.' uf I~ uc or this 1.:ompany or any mcmbct· ofits statl~ 1..1r r'-'PI\ldll~tion uf this report in ~unnt'ction with th~ lUh ~..·rtisem"·nt, promotion or sate ul' any prodm:l orprnccss. or ln conn~..·ctiun with thL· re-puhlkutiun ~lr thi~ rcpnrt for any rurp..ls.t.: otht."r than tilr th~..: ud.tln:ss~\.· will h~: g.runt~.:U '"mly on contact Thi~ American West Analytical Laboratories UL Denison WORK ORDER Summary WorkOrder: 1310621 Page 1 of2 Client: Energy Fuels Resources, Inc. Due Date: 1111112013 ClientiD: DEN100 Contact: Garrin Palmer Project: 4th Quarter Chloroform 2013 QC Level: III WO Type: Project Comments: PA Rush. QC 3 (Summary/No chromatograms). RL of 1 ppm for Chloride and VOC and 0.1 ppm for N02/N03. Expected levels provided by client-see Jenn. J-flag what we can't meet. ElM Locus and EDD-Denison. Email Group.; ~ Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage l310621-001A MW-32_10292013 10/29/2013 1330h 10/31/2013 0935h 300.0-W Aqueous ~ elf-we I SELAnalytes: CL 1310621-001B N02/N03-W-353.2 ~ elf-no2/no3 1 SEL Analytes: N03N02N 1310621-001C 8260-W ~ VOCFridge Test Group: 8260-W-Custom; #of Analytes: 4 I# of Surr: 4 l310621-002A TW4-25_10292013 10/29/2013 1204h 10/31/2013 0935h 300.0-W Aqueous ~ elf-we 1 SELAnalytes: CL 1310621-002B N02/N03-W-353.2 0 elf-no2/no3 1 SEL AnaJytes: N03N02N 1310621-002C 8260-W 0 VOCFridge 3 Test Group: 8260-W-Custom; #of Analytes: 41 # ofSurr: 4 1310621-003A TW4-24_10292013 10/29/2013 1220h 10/31/2013 0935h 300.0-W Aqueous 21 elf-we ·I 1 SEL Analytes: C~ 1310621-00JB N02/N03-W-353.2 ~ elf-no2/no3 1 SEL Analytes: N03N02N 1310621-003C 8260-W ~ VOCFridge Test Group: 8260-W-Custom; #of Analytes: 4 I# ofSurr: 4 1310621-004A TW4-04_10292013 10/29/2013 1302h I 0/31/2013 0935h 300.0-W Aqueous ~ df-wc I SELAnalytes: CL 1310621-004B N02/N03-W-353.2 21 elf-no2/no3 1 SEL Analytes: N03N02N l310621-004C 8260-W ~ VOCFridge 3 Test Group: 8260-W-Custom; #of Analytes: 4 I# ofSurr: 4 1310621-00SA MW-04_10292013 10/29/2013 1255h 10/31/2013 0935h 300.0-W Aqueous 21 df-wc 1 SEL Analytes: CL 1310621-00SB N02/N03-W-353.2 0 elf-no2/no3 I SEL Analytes: N03N02N 1310621-00SC 8260-W ~ VOCFridge 2 Test Group: 8260-W-Custom; #of Analytes: 41# ofSurr: 4 131 0621-006A MW-26_10292013 10/29/2013 1246h 10/31/2013 0935h 300.0-W Aqueous ~ df-wc 1 SEL Analytes: CL %M ~ RT ilY' CN I?" TAT []7 QC fB7 ? Printed: 11/1/2013 FOR LABORATORY USE ONLY [fill out on page 1]: HOK __ HOK __ HOK __ COC Emailed WORK ORDER Summary WorkOrder: 1310621 Page 2 of2 Client: Energy Fuels Resources, Inc. Due Date: 1111112013 SampleiD Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1310621-0068 MW-26 _ _10292013 10/29/2013 1246h 10/31/2013 093 Sh N02/N03-W-353.2 Aqueous ~ df-no2/no3 1 SEL Analytes: N03N02N 131 0621-006C 8260-W ~ VOCFridge 3 Test Group: 8260-W-Custom; #of Analytes: 4/ # ofSurr: 4 1310621-007A TW4-19 ... 10292013 10/29/2013 1410h 10/31/2013 0935h 300.0-W Aqueous ~ df-wc 1 SEL Analytes: CL 1310621-007B N02/N03-W-353.2 ~ df-no2/no3 1 SEL AnQiytes: N03N02N 1310621-007C 8260-W ~ VOCFridge 3 Test Group: 8260-W-Custom; #of Analytes: 4/ # ofSurr: 4 131 0621-008A TW4-22_10292013 10/29/2013 1227h 10/31/2013 0935h 300.0-W Aqueous ~ df-wc r 1 SEL Aoolyt~s: CL 1310621-0088 N02/N03-W-353.2 ~ df-no2/no3 1 SEL Analytes: N03N02N 1310621-00SC 8260-W ~ VOCFridge 3 Test Group: 8260-W-Custom; # of Analytes: 4/ #of Surr: 4 1310621-009A TW4-20_10292013 10/29/2013 1240h 10/3112013 0935h 300.0-W Aqueous !Jl df-wc 1 SEL A,nalyces: CL 1310621-0098 N02/N03-W -353.2 ~ df-no2/no3 1 SEL A11alyt~: N03N02N 131 0621-009C 8260-W 0 VOCFridge 3 Test Group: 8260-W-Custom; #of Analytes: 4/ # ofSurr: 4 1310621-0lOA TW4-65_10292013 10/29/2013 1330h 10/31/2013 0935h 300.0-W Aqueous ~ df-wc I SEL Analytes: CL 1310621-0lOB N02/N03-W-353.2 ~ df-no2/no3 I SEL A,ll(llyies: N03N02N 1310621-010C 8260-W 0 VOCFridge 3 Test Group: 8260-W-Custom; #of Analytes: 4/ # ofSurr: 4 1310621-0llA Trip Blank 10/2912013 10/31/2013 0935h 8260-W Aqueous ~ VOCFridge 3 Test Group: 8260-W-Custom; #of Analytes: 41# ofSurr: 4 Printed: 11/1/2013 FOR LABORATORY USE ONLY [fill out on page 1): %M 0 RT 0 CN 0 TAT 0 QCO HOK __ HOK __ HOK___ COC Emailed,__ ___ _ CLIENT: ADDRESS: CONTACT: PHONE#: AMERICAN WEST ANALYTICAL LABORATORIES 463 W. 3600 S. SA!.T LAKE CiTY. UT 84115 PHONE It (801) 2G3-68S6 TOLL FREE# (668) 263-6666 FAX It (801) 263-8687 EMAIL AWAL@AWAL-LABS.COM WWW .AWAL-LABS.COM Energy Fuels Resources, Inc- 6425 S. Hwy. 191 Blanding, UT 84511 Garrin Palmer (435) 678-2221 CELL#: -,,-pa=lm::--...,--,@e,-n_e_r_gy=fa,...e-,ls;-.c-om--;..-KW='""eln;-el@e"' nere;y"'fu""els=-.c-o.,..m::--; -------- CHAIN OF CUSTODY ALL ANALY8lS WILL BE CONDUCToeD USING NELAP AC:CRE!DIUD MeTHODS AND ALL DATA WIU. Bl! REPORTI!D USINCJ AWAL's STANDARD ANALYTI! USTS AND REPORTING UMrrs {PQL) UNLJ!!SS SP!!CIPICALLY REaUf!STED OTHBRWISI! ON THIS CHAJN OP CUSTODY AND/OR ATTACHI!D DOCUMENTATION \~ \0&:>2\ A W AL LAB SAMPLE SET # PAGE 1 OF 1 ~~J TURN AROUND TiM&: UNLESS OT'HI!R A.RA.ANGBMI!INTS HAVI II DUB DATE: STANDARD BI!I!N MAD!:, SIGINI!D RI!PORTS WIU. •• I!MAILI!ID DY 5:00 PM ON THE DAY THEY ARI! DUE. X INCLUDE EDD: LOCUS UPLOAD EXCEL FIELD FILTERED FoR: LABORATORY USE ONLY .li;AMI'UIO W~R&; ()-...£5 ~~No oeuve.ReD 1 2 AMBIBNT O~ FOR COMPLIANCE WITH: . ~ 0 NELAP 3 TeMPI!RATURa ~ •c EMAIL: dmrk@om.ere;yfuels.eom PROJECT NAME: 4th quarter chloroform 2013 PROJECT#: "' a: >< .. c:< ~ C' a 0 RCRA 0 CWA 0 SDWA 0 ELAP I A2LA 0 NLLAP 0 NoN-COMPUANCE 0 OTHER: 4 Reci!UVED BROKI!N/Le:AKINCJ~ ~ (:)ROPIIRLY~ -('\ -~I .1 · \13 VG \II 5 PJtoP!IRLY PRE&BAVRD b ~~ y N PO#: SAMPLER NAME: Tanner Holliday SAMPLE 10: DATE SAMPLED MW-32_10292013 I \0./"Z.q) 1'3 :z: it ~ ... z ~ 0 u Ill .J !2. (') 0 II: TIME I~ 0. :l: <( SAMPLED :o:. Ill s 12: 1330 5 IW X a D' (T) .._ a 0 10 a ~ 5l ~ :t. .. 0 0 0 > X X KNOWN HAZARDS & SAMPLE COMMENTS CHecKI!D AT I!II!!NCH y N 6 Re:ci!!IVBD WrrHIN ~TIMES L/ N ITW4-25 10292013 \D/2"\ I \3 1204 5 w X X X coc TAPB WAll: l~NT ON OUTIIR PACKAOB TW4-24 ~029201.3 10/lVI3 1220 5 w X X X 0 N NA TW4-04~10292013 l0{2q/l:) 1302 5 w X X X . . -~J<JIN ON OUTBR PACKAGIE · O~\lcr_ Vln.\ ~.eweo v N NA 1MW-04 10292013 \OJ2.'!/\.:!> 1255 5 W X X X .V)Yr-1\u)i'\. 3 PRI!&ENT~Pt.a MW-.26 .102920~3 \0/Z'l./ \3 1246 5 W X X X y 6 NA TW4-19_10292013 \0/14/1.3 1410 5 w X X X 4 UNBROKON ON Siul~· I Y N NA TW4-22_~0292013 tr>h.'J/I":> 1227 6 W X X X TW4-20_1~013 I I0/"2.'1/]:3 I 1240 15 IW I X I X I X TW4-. 65_10292013 OISCR!PANCIBS S15SAMPL!! t=r.~~~~:c~-------------------------------l~~~~--t-~:::_-i~~~~i-~~~~-+--~--t---t-~~-4--~--~~~---------------------'IL-aouANococR 7 -rrl~ ~'k v N - ~ti1o RlMk I I I 1 l:v-1 I R•~ulliKI!D ·~ J 1 lid. / (DATe: !>,.... .. ,........ --J~ J-1;;-{b~ I0}3o/J3 ~CJli'V.ao BY: SxtHA.TUR.11 / DATE: Sl'eCIAL INSTRUCTIONS: p,,.,. N......, ....-r:;:nn.:r lfol liJ~~J l~'"'i2oo 1:M N..,.., / 'TIMe: R•nJiicov'-">-..Y; · ---~ ------·· DATE: I See the Analytical Scope of Work for Reporting Limits and SICJNATuRe VOC analyte list. TIME: PA1tn N.A.wtl ,Recerveo BY: SIGNATURE o .. .,.,.~ Rlu.o<<wwnoo 10v: S.N1MA.nnm [DAre: PIUJ<1 N .. LIII! /\ PU..U,.NANto ~: TIMB: DAte: 7 DATI!: R•c•JVeoav:J..'jn ~ SI<:INATURE! X ' ~Ul:CiotW,n BY: G~..,1,.TUP..1 l~.l'5 \l l3 PRINT NAMe: ~_hL~C'lJ...LLV\. PRINT NAME: /r 1TIME!: T"-'"' <*~~~ A W AL -Analytical Scope of Work White Mesa Mill Blanding Utah Page 11 of 13 An~Jytrfml ReJ?ort:ing .Maximum Sample-iSamp~(} Metl;lod ·· imje' FtoldiiJ.g Preservatioo r ootperaft.n:e .... ,; , ro ... be ·useW 1 , · · ;i:'ua~~ Req_lliremet;t.ts Re<:(niiements A45~--rfug!L 2~ None ~~:!or ~ Sulfate -----E300.0 I -----Carbon~03 A2320 B 1 mg!L 14 days None ~bonate as HC03 A2320 B 1 mg!L 14 days None Volatile ()rgar:U9 Coll;J,ponn~~hloroform Pio[!;ram •. Carbon Tetrachloride SW8260B 1.0 11g/L 14 days HCl to pH<2 Chloroform Diehl oro methane (Methylene Chloride) Chloromethane or SW8260C SW8260B or SW8260C SW8260B or SW8260C SW8260B or SW8260C 1.0 llg!L 1.0 llg/L 1.0 ~-tg!L 1 2,~chlorobenzene SW8270D <10 ug/L 1,2-DichfONl:>enzene SW8270D <10 ug!L 1,3-Dichlorobemene SW8270D <10 ug!I, I 4-Dichlorobenzen~ SW8270D <10 ug/L 1-Methylnaphthalene ~ SW8270D <10 ug/L 2,4,5-Trichlorophenol ~8270D . <1 0 ug/L 2,4,6-Trichloropheno1 SWrnQD <10 ug!L 2,4-Dichloropheno1 SW8270J:)'-. <1 0 ug/L 2,4-Dimethylphenol SW8270D <~giL 2.4-Dinitrophenol SW8270D <20 u~ 2,4-Dinitroto1uene SW8270D <...J,.e""ug/L 2 6-Dinitrotoluene SW8270q ....... <10 ug/L 2-Ch1oronaphtha1ene SWS).?{JD <10 ug/L 2-Chloropheno1 _s.W"8270D <1 0 ug/L 2-Methylnaphthalene / SW8270D <10 u_g/L 2-Methy1phenol / SW8270D <1 0 u_g/L 2-Nitropheno1 /' SW8270D <10 ug/L 3&4-Meth~eno1 SW8270D <10 ug/L ~3 '-.Dk@orobenzidine SW8270D <1 0 ug&_ 4$-binitro-2-methy1phenol SW8270D <10 ug!L 14 days HCl topH<2 ::S6°C 14 days HCl to pH<2 ::S6°C 14 days HCI to pH<2 ::S6°C 7/40 days None <pC 7/40 days None ,......v < 6°C 7/40 days Non.V < 6°C 7/40 days _N6ne < 6°C 7/40 days / None < 6°C 7/40 da~ None < 6°C 7/4.0-'fiays None < 6°C /1740 days None < 6°C 7/40 days None < 6°C ~40 days None < 6°C 7/40 da~ None < 6°C 7/40 days ~None < 6°C 7/40 days ~e < 6°C 7/40 days None~ < 6°C 7/40 days None -........ < 6°C 7/40 days None < 6~ 7/40 days None < 6°C ~ Analysis Ammonia COD Cyanide Metals NOz&N03 O&G Phenols Sulfide TKN TP04 Procedure: Frequency: Preservation Check Sheet s ---le Set E --- Preservative -oo\ -ooL--CO"~ --co-\ i:-tb CCh pH <2 H2S04 pH <2 H2S04 pH>12 NaOH pH<2HN03 pH <2 fhS04 b.J-e7 Jp_~ r,l ()_?:J V£0 ves \lz.-S pH<2HCL I ' r I I I' pH<2 H2S04 pH>9NaOH, Zn Acetate _pH <2H2S04 pH<2 H2S04 Pour a small amount of sample in the sample lid Pour sample from Lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid -COl 1\J~S I -dnH ·-cos-·mer 1\le~ 1\/£S ( Jf -010 \/£-5. f 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + .... # • The sample required additional preservative upon receipt. The sample was received unpreserved The Sample was received unpreserved and therefore preserved upon receipt The sample pH was unadjustable to a pH < 2 due to the sample matrix The sample pH was unadjustable to a pH > __ due to the sample matrix interference Lab Set ID: \ ~ '\ Ok?2 \ 463 West 3600 South 3alt Lake City, UT 84115 Phone: (80 1) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Garrin Palmer Energy Fuels Resources, Inc. 6425 S. Hwy 191 Blanding, UT 84511 TEL: ( 435) 678-2221 RE: 4th Quarter Chloroform 2013 Dear Garrin Palmer: Lab Set ID: 1311306 American West Analytical Laboratories received 16 sample(s) on 11115/2013 for the analyses presented in the following report. American West Analytical Laboratories (AWAL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. This is a revision to a report originally issued 11126/2013. Pages 1-3, 20, and 35 have been updated. Thank You, I Kyle F Digitally signed by Kyle F Gross Cl~ cn=Kyle F. Gross, o=AWAL, II!'•AWAI..-I.Jil>ct~TOI'f Director, omoU•kyie@uwn~l!l~ c=US 01)'1 : 20'1m04 15:10:27 -07'00' Gross Approvedby: ~------=·~--------------~ Laboratory Director or designee Report Date: 12/4/2013 Page I of 45 All analyse.s llpplicoblc to the CWA. SDWA, and RCRA nre pcrfom1ed in ,occordance to NELAC protocols Pertinent sampling in formation is located on the aUnchcd COC Confidential Businc5s Infonnalion: This rcpor1 is prO\'idcd fur I he e:<c\u!:livc usc of lhe ~lldresscc Pri,·iJe~cs o! sub;~cq~cnt ~~c oflhc ~~',llc of this .con~pnny or any D_!.7mhcr of ils staff, orrcproduclio~ ~f lhis rcpo~ in ~on~cction~ with the a~vcrtiscn;cnl, p:omolio.n or sale or?~Y. ~rod~ct or P~?ccss, ~r in :onn~c~ion w~th th~ n;·publicalion ofthi.s n:por' SAMPLE SUMMARY Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer • Project: 4th Quarter Chloroform 2013 Lab Set ID: 1311306 Date Received: 11115/2013 0850h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 463 West 3600 South 1311306-001A TW4-06 11132013 11 /13/2013 0700h Aqueous Anions, E300.0 ;alt Lake City, UT 84115 1311306-00 1B TW4-06 11132013 11113/2013 0700h Aqueous Nitrite/Nitrate (as N), E353.2 1311306-001C TW4-06 11132013 11/13/2013 0700h Aqueous VOA by GC/MS Method 8260C/5030C Phone: (80 1) 263-8686 1311306-002A TW4-05 11132013 11/13/2013 0708h Aqueous Anions, E300.0 1311306-002B TW4-05_11132013 11113/2013 0708h Aqueous Nitrite/Nitrate (as N), E353.2 Toll Free: (888) 263-8686 1311306-002C TW4-05 11132013 11113/2013 0708h Aqueous VOA by GC/MS Method Fax: (801) 263-8687 8260C/5030C !-mail: awal@awal-labs.com 1311306-003A TW4-18 11132013 11/13/2013 0718h Aqueous Anions, E300.0 1311306-003B TW4-18 11132013 11 /13/2013 0718h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 1311306-003C TW4-18_11132013 11113/2013 0718h Aqueous VOA by GC/MS Method 8260C/5030C 1311306-004A TW4-21_11132013 11113/2013 0723h Aqueous Anions, E300.0 Kyle F. Gross 1311306-004B TW4-21 11132013 11113/2013 0723h Aqueous Nitrite/Nitrate (as N), E353.2 1311306-004C TW4-21_11132013 11113/2013 0723h Aqueous VOA by GC/MS Method Laboratory Director 8260C/5030C 1311306-005A TW4-29 11132013 11113/2013 0737h Aqueous Anions, E300.0 Jose Rocha 1311306-005B TW4-29_11132013 11113/2013 0737h Aqueous Nitrite/Nitrate (as N), E353.2 QA Officer 1311306-005C TW4-29_11132013 11113/2013 0737h Aqueous VOA by GC/MS Method 8260C/5030C 1311306-006A TW4-11_11132013 11113/2013 0745h Aqueous Anions, E300.0 1311306-006B TW4-11_11132013 11 /13/2013 0745h Aqueous Nitrite/Nitrate (as N), E353 .2 1311306-006C TW4-11 11132013 11113/2013 0745h Aqueous VOA by GC/MS Method 8260C/5030C 1311306-007 A TW4-07_11142013 11114/2013 0813h Aqueous Anions, E300.0 1311306-007B TW4-07 11142013 11114/2013 0813h Aqueous Nitrite/Nitrate (as N), E353.2 1311306-007C TW4-07_11142013 11114/2013 0813h Aqueous VOA by GC/MS Method 8260C/5030C 1311306-008A TW4-10_11142013 11/14/2013 0820h Aqueous Anions, E300.0 1311306-008B TW4-10_11142013 11/14/2013 0820h Aqueous Nitrite/Nitrate (as N), E353.2 1311306-008C TW4-10_11142013 11/14/2013 0820h Aqueous VOA by GC/MS Method 8260C/5030C 1311306-009A TW4-01_11142013 11114/2013 0828h Aqueous Anions, E300.0 1311306-009B TW4-01_11142013 11/14/2013 0828h Aqueous Nitrite/Nitrate (as N), E353.2 1311306-009C TW4-01_11142013 11114/2013 0828h Aqueous VOA by GC/MS Method 8260C/5030C 1311306-010A TW4-02_11142013 11114/2013 0833h Aqueous Anions, E300.0 1311306-010B TW4-02 11142013 11/14/2013 0833h Aqueous Nitrite/Nitrate (as N), E353.2 Report Date: 12/4/2013 Page 2 of 45 All analyses applicable to the CWA, SDWA. and RCRA ure rerfom1ed in accordance to NELAC protocols Pertinent 5ampling infom1alion is locateU on tho:: attached COC Confidential Business lnfommtion: This n:rort is provided for the exclusive usc of the addressee Pri\'ilcgcs of subsequent usc of the name of this com(l<my or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-public~tion or this rcpor -. . .. . . . .. . . . ...... . .. ... ~ . . -~ . . . . . ~ . . .. . . .. . ' . - Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Project: 4th Quarter Chloroform 2013 Lab Set ID: 1311306 Date Received: 11115/2013 0850h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 1311306-01 oc TW4-02 11142013 11114/2013 0833h Aqueous VOA by GC/MS Method 463 West 3600 South 8260C/5030C 1311306-011A TW4-32_11142013 11/14/2013 0842h Aqueous Anions, E300.0 3alt Lake City, UT 84115 1311306-0llB TW4-32 11142013 11114/2013 0842h Aqueous Nitrite/Nitrate (as N), E353.2 1311306-011C TW4-32 11142013 11/14/2013 0842h Aqueous VOA by GC/MS Method 8260C/5030C 1311306-012A TW4-33 11142013 11/14/2013 0849h Aqueous Anions, E300.0 Phone: (80 1) 263-8686 1311306-012B TW4-33 11142013 11/14/2013 0849h Aqueous Nitrite/Nitrate (as N), E353.2 Toll Free: (888) 263-8686 1311306-012C TW4-33 11142013 11114/2013 0849h Aqueous VOA by GC/MS Method Fax: (80 1) 263-8687 8260C/5030C ~-mail: awal@awal-labs.com 1311306-013A TW4-34 11142013 11/14/2013 0856h Aqueous Anions, E300.0 1311306-013B TW4-34_11142013 11/14/2013 0856h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 1311306-0BC TW4-34 11142013 11/14/2013 0856h Aqueous VOA by GC/MS Method 8260C/5030C 1311306-014A TW4-60 11142013 11/14/2013 0700h Aqueous Anions, E300.0 1311306-014B TW4-60 11142013 11/14/2013 0700h Aqueous Nitrite/Nitrate (as N), E353.2 Kyle F. Gross 1311306-014C TW4-60 11142013 11/14/2013 0700h Aqueous VOA by GC/MS Method Laboratory Director 8260C/5030C 1311306-015A TW4-18R 11122013 * 11/12/2013 0827h Aqueous Anions, E300.0 Jose Rocha 1311306-015B TW4-18R_11122013 * 11112/2013 0827h Aqueous Nitrite/Nitrate (as N), E353.2 QA Officer 1311306-015C TW4-18R 11122013 * 11/12/2013 0827h Aqueous VOA by GC/MS Method 8260C/5030C 1311306-016A Trip Blank 11/12/2013 Aqueous VOA by GC/MS Method 8260C/5030C * -Reissue of a previously generated report. The Client Sample ID has been updated. Information herein supersedes that of previously issued reports. Report Date: 12/4/2013 Page3 of45 AIIDnalyses applicable to the CWA, SDWA, and RCRA arc pcrfonncd in accordance to NELAC protocols Pertinent sampling infonmtion is located on the attached COC. Contidcntial Business Jnfo•mation: This 1\!I)On is provided tOr the exclusive usc of the ~ddrcsscc P1ivilc~cs o: :;mbrscq~ent ~~c of the ~~~c of this .con~pany or any ~:mbcr of its s.laff, or rcproLiuclio~ ~fthis rcpo~ in ~on~cction_ with I he a~~crtisc~lcnl, p!omotio.n or Sillc of ?~Y ~10d~ct or f.l~?<=css, (;r in :onn~c~ion w~th th~ r:·publication of this n:poT1 463 West 3600 South )alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Garrin Palmer Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: 4th Quarter Chloroform 2013 1311306 11115/2013 11/12, 11113, & 11114/2013 Intact None Holding Time and Preservation Requirements: The analysis and preparation for the samples were performed within the method holding times. The samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, DUP: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exceptions: The MS percent recoveries were outside of control limits on nitrate/nitrite for samples 1311306-001 B and -007B due to sample matrix interference. Duplicate (DUP): The parameters that required a duplicate analysis had RPDs within the control limits. Corrective Action: None required. Report Date: 11126/2013 Page 4 of 45 All analyses upplicable to the CWA, SOWA, and RCRA are performed in accordance to NELAC protocoh. Pertinent sampling informlltion is louted on the aUachcd COC Coutidenti-.1 Bu:-.incss Information: This report is provided for the exclusive usc of the ~ddn!sscc, Privilc~cs o: sub .. scq~ent ~~c of the ~?~c of this .con~pany or nny ·~:~1bcr of its staff. or rcproductio~ ~fthis rcpo'!: in ~on?cctiOT~ wi1h the a~vcrtiscn_tcnt. r;~motio.n o.r ~ale or ~~Y. ~rod~cl or P~?ccss, ~r in :onn:c~ion w!th th~ r:-publicalion of this report 463 West 3600 South )alt Lake City, UT 84115 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 1) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Kyle F. Gross Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Energy Fuels Resources, Inc. Garrin Palmer Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date(s) of Collection: Sample Condition: C-0-C Discrepancies: Method: Analysis: 4th Quarter Chloroform 2013 1311306 11/15/2013 11/12, 11113, & 11114/2013 Intact None SW-846 8260C/5030C Volatile Organic Compounds General Set Comments: Multiple target analytes were observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Sun·ogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike I Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 11/26/2013 Page 5 of45 All analyses applicob\c to the CWA, SDWA, und RCRA arc performed in accordance to NELAC protocols Pertinent sampling information is located on the attnchcd COC Con1idcntial Business Jnfonnation: This report is provided for the exclusive usc ufthc ~Utlrcsscc Privilc~cs u.r sub~scq~cnl ~~c of the ~~~c of I his .con!pany or nny n.2.~mbcr of its staff. or rcproductio~ ~flhis rcpo~ in ~on?ection~ with I he a.~vcrtisc~uml. p~tnnolio.n ~r ~ale or~~y ~rod~cl or p~occss, ~r in ~onn:_c~ion with th; r:-puhlication oflhis rcpur1 Client: Energy Fuels Resources, Inc. LabSetiD: 1311306 Project: 4th Quarter Chloroform 2013 Analyte Result Units 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Q_C_SUMM_ARY. REP_QR_T_ Contact: Garrin Palmer Method MDL Reporting Limit Dept: we QCType: DUP Amount Spiked Spike Ref. Amount %REC Lab Sample ID: 1311161-013BDUP DateAnalyzed: 11/15/2013 1742h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.33 mg/L E353.2 0.00252 0.100 Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual 1.3 1.94 20 Report Date: 11/26/20 13 Page 3 7 of 45 l analyses applicable to the CWA, SDWA, and RCRA arc performed in accordance to NELAC protocols_. Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive usc of the addressee. Privileges of subsequent usc oft~ ue oftl1is company or any member of its staff, or reproduction of this report in connection with tht! advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be !::,'TUntcd only on contact, This Client: Energy Fuels Resources, Inc. Lab Set ID: 1311306 Project: 4th Quarter Chlorofonn 2013 Analyte Result Lab Sample ID: LCS-R61996 Date Analyzed: Test Code: 300.0-W Chloride 4.58 Lab Sample ID: LCS-R61712 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 0.978 Lab Sample ID: LCS-R61713 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.03 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: ¥/WW.awal-labs.com _QC SUMMARY REPORT Contact: Garrin Palmer Dept: we Units Method 11/22/2013 0137h mg/L E300.0 11/15/2013 1708h mg/L E353.2 11115/2013 1851h mg/L E353.2 MDL 0.0114 0.00252 0.00252 Reporting Limit 0.100 0.100 0.100 QC Type: LCS Amount Spiked 5.000 1.000 1.000 Spike Ref. Amount 0 0 0 %REC 91.6 97.8 103 Limits 90-110 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 11/26/2013 Page 38 of 45 ! analyses applicable to the CWA, SDWA, and RCRA arc pcrfonncd in acco1dancc to NELAC protocoi::L Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive usc of the addressee Privileges of subsequent usc ofth 11e of this company or any member of its staff, or n::procluction of this report in connection with tht! advc11iscment, promotion 01· sale of any product or process, or in connection with the re-publication of this report for any purt)ose other than for the addressee will be grantt•d only on contact This Client: Energy Fuels Resources, Inc. Lab Set ID: 1311306 Project: 4th Quarter Chloroform 2013 Analyte Result Lab Sample ID: MB-R61998 Date Analyzed: Test Code: 300.0-W Chloride <0.100 Lab Sample ID: MB-R61712 Date Analyzed: Test Code: N02fN03-W-353.2 NitratefNitrite (as N) <0.100 Lab Sample ID: MB-R61713 Date Analyzed: Test Code: N02fN03-W -353.2 NitratefNitrite (as N) <0.100 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com Q_C_ SU_MMARY_RE~ORI_ Contact: Garrin Palmer Dept: we QC Type: MBLK --- Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 11/22/2013 0113h mg!L E300.0 0.0114 0.100 11/15/2013 1706h mg/L E353.2 0.00252 0.100 11/15/2013 1849h mg/L E353.2 0.00252 0.100 Limits Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPD Limit Qual Report Date: 11/26/2013 Page 39 of 45 ! analyses applicable to the CWA, SDWA, and RCRA arc pcrfonn~.::d in accordance to NELAC protocols~ Pertinent sampling information is located on the attached COC Contidcntial Business Information: This report is pi'Ovidcd for the exclusive w;c of the add1csscc. Privileges of subsequent usc of th ne of this company or any member of its staft~ or reproduction of this rcporl in connection with tht:: advertisement, promolion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for tht: addressee will be .!Zfantcd only on contacl. This 463 West 3600 South Salt Lake City, UT 84115 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC _S_UMMARY RElQRI_ Client: Energy Fuels Resources, Inc. Lab Set ID: 1311306 Project: 4th Quarter Chloroform 2013 ----- Analyte Result Units Method MDL Lab Sample ID: 1311306-0ISAMS Date Analyzed: 11/22/2013 0403h Test Code: 300.0-W Chloride 4.76 mg/L E300.0 0.0114 Lab Sample ID: 1311306-00lBMS Date Analyzed: 11/15/2013 1717h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 10.4 mg/L E353.2 0.0252 Lab Sample ID: 1311306-007BMS Date Analyzed: 11/15/2013 1746h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 15.4 mg/L E353.2 0.0252 Lab Sample ID: 1311306-0lSBMS Date Analyzed: 11115/2013 1853h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.01 mg/L E353.2 0.00252 1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Reporting Limit 0.100 1.00 1.00 0.100 Contact: Garrin Palmer Dept: we QCType: MS Amount Spiked 5.000 10.00 10.00 1.000 Spike Ref. Amount 0 1.52 4.13 0 %REC 95.1 89.2 113 101 Limits 90-110 90-110 90-110 90-110 Kyle F. Gross Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual ReportDate: 11/26/2013 Page40of45 ; analyses applicable to the CWA, SDW A, aml RCRA arc pcrf01 mcd in ac~;oJ dance 10 NELAC protocols .. Pcr1incnt sampling info1mation is located on the attached COC. Confidential Business lnfonnation: This report is providl!d for thC' exclusive usc of the add1c~cc Privileges of subsequent usc of th nc of this company or any member of its staff, or rcp1oduction of this report in connection with the advertisement, promotion or sale of any product or process. or in connection willt the re-publication of this report for any purpose olher than for the addressee wi11 be &rranlcd only on contact. This 463 West 3600 South Salt Lake City, UT 84115 Kyle F. Gross Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer _QC_SJIMMAR.Y_REP_QRI_ Client: Energy Fuels Resources, Inc. Contact: Garrin Palmer Lab Set ID: 1311306 Dept: we Project: 4th Quarter Chloroform 2013 QC Type: MSD ------~ -~ ---- Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt ~oRPD Limit Qual Lab Sample 10: 1311306-015AMSD Date Analyzed: 11/22/2013 0427h Test Code: 300.0-W Chloride 4.81 mg/L E300.0 O.otl4 0.100 5.000 0 96.1 90-110 4.76 1.07 20 Lab Sample 10: 1311306-00lBMSD Date Analyzed: 11/15/2013 1719h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 11.3 mg/L E353.2 0.0252 1.00 10.00 1.52 97.6 90-110 10.4 7.77 10 -Lab Sample ID: 1311306-007BMSD Date Analyzed: 11/15/2013 1748h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 15.1 mg/L E353.2 0.0252 1.00 10.00 4.13 110 90-110 15.4 2.29 10 Lab Sample 10: 1311306-01SBMSD Date Analyzed: 11/15/2013 1855h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.03 mg/L E353.2 0.00252 0.100 1.000 0 103 90-110 1.01 1.42 10 Report Date: II /26/20 13 Page 41 of 45 :analyses applicabJc to the CWA. SDWA, W1d RCRA arc p~:rformcd in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC. Contidcnrial Business Information: This report is provided for the exclusive usc of the addressee Privileges of subsequent usc ofth 11e of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than fm the addressee will be granted only on contact, This American West Analytical Laboratories REVISED: 12/3/2013 UL Denison #15 Sample ID corrected -RW WORK ORDER Summary WorkOrder: 1311306 Due Date: 11126/2013 Page I of3 Client: Client ID: Project: Comments: SampleiD 1311306-001A 1311306-001 B 1311306-001 c 1311306-002A 1311306-002B 1311306-002C 1311306-003A 1311306-003B 1311306-003C 1311306-004A 1311306-004B 1311306-004C 1311306-005A 1311306-00SB 1311306-00SC Printed: 12/3/2013 Energy Fuels Resources, Inc. DEN100 Contact: Garrin Palmer 4th Quarter Chloroform 2013 QC Level: III WO Type: Project PA Rush. QC 3 (Summary/No chromatograms). RL of 1 ppm for Chloride and VOC and 0.1 ppm for N02/N03. Expected levels provided by client-see Jenn. J-flag what we can't meet. ElM Locus and EDD-Denison. Email Group.; Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage TW4-06_11132013 11113/2013 0700h 11/15/2013 0850h 300.0-W Aqueous [;;'] df-wc I SEL Analytes: CL N02/N03-W-353.2 [~] df-no2/no3 I SEL Ana/ytes: N03N02N 8260-W VI VOCFridge Test Group: 8260-W-Custom; # Q[ Analytes: 4 I# Q[Surr: 4 TW4-05_11132013 11/13/2013 0708h 11 /15/2013 0850h 300.0-W Aqueous [~1 df-wc I SEL Analytes: CL N02/N03-W-353.2 ["I df-no2/no3 I SEL Alla~\lles; N03N02N 8260-W 1-tl VOCFridge Test Group: 8260-W-Custom; #of Analytes: 4 I # ofSurr: 4 TW4-18_11132013 11/13/2013 0718h 11/15/2013 0850h 300.0-W Aqueous l~J df-wc I SEL Analytes: CL N02/N03-W-353.2 ~J df-no2/no3 I SEL Ana/ytes: N03N02N 8260-W [~1 VOCFridge Test Group: 8260-W-Custom; #of Analytes: 4 I # of Surr: 4 TW4-21_11132013 11/13/2013 0723h 11/15/2013 0850h 300.0-W Aqueous I~ df-wc I SEL Analytes: CL --N02/N03-W-353.2 ~J df-no2/no3 I SEL Analytes: N03N02N 8260-W ~I VOCFridge Test Group: 8260-W-Custom; #of Ana lyles: 4 I# o.fSurr: 4 TW4-29_11132013 11/13/2013 0737h 11/15/2013 0850h 300.0-W Aqueous ~I df-we 1 SEL Analytes: CL N02/N03-W-353.2 1~1 df-no2/no3 __ I SEL Atmlytf!s.: N03N02N 8260-W ,v VOCFridge Test Group: 8260-W-Custom; #of Ana~ytes: 4 I # ofSurr: 4 3 3 3 WORK ORDER Summary Work Order: 1311306 Page 2 of3 Client: Energy Fuels Resources, Inc. Due Date: 11126/2013 Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1311306-006A TW4-11_11132013 11113/2013 0745h 11/15/2013 0850h 300.0-W Aqueous 1~1 df-we 1 SEL Analytes: CL ----1311306-0068 N02/N03-W-353.2 I~J df-no2/no3 I SEL Analytes: N03N02N 1311306-006C 8260-W l~l VOCFridge 3 Test Group: 8260-W-Custom; # ~f Ana/ytes: 4 I # ~f Surr: 4 1311306-00?A TW4-07_11142013 11/14/2013 0813h 11/15/2013 0850h 300.0-W Aqueous l;fl df-wc I SEL Analytes: CL 1311306-0078 N02/N03-W-353.2 I~ I df-no2/no3 I SEL .4.nafytes; N03N02N 1311306-00?C 8260-W lvl VOCFridge Test Group: 8260-W-Custom; #of Analytes: 4 I# of Sw7': 4 1311306-00SA TW4-10_11142013 11/14/2013 0820h 11/15/2013 0850h 300.0-W Aqueous IY'l df-wc I SEL Analytes: CL 1311306-0088 N02/N03-W-353.2 ~1 df-no2/no3 I SEL Analytes: N03N02N 1311306-00SC 8260-W ~ VOCFridge 3 Test Group: 8260-W-Custom; #of Analytes: 4 l #ojSurr: 4 1311306-009A TW4-01_11142013 11/14/2013 0828h 11/15/2013 0850h 300.0-W Aqueous [vi df-wc 1 SEL Analytes: CL 1311306-0098 N02/N03-W-353.2 1~1 df-no2/no3 1 SEL Analytes: N03N02N 1311306-009C 8260-W I~ I VOCFridge 3 Test Group: 8260-W-Custom; #of Ana(vtes: 4 I# ofSurr: 4 1311306-0lOA TW4-02_11142013 11/14/2013 0833h 11/15/2013 0850h 300.0-W Aqueous ~] df-wc 1 SEL Analytes: CL 1311306-0108 N02/N03-W-353.2 !Vl df-no2/no3 1 SEL Analytes: N03N02N 1311306-0IOC 8260-W [.;(I VOCFridge Test Graue,: 8260-W-Custom; #of Ana lyles: 4 I # ~(Surr: 4 1311306-011A TW4-32_11142013 11/14/2013 0842h 11/15/2013 0850h 300.0-W Aqueous I~ I df-wc 1 SEL Anal tes: CL 1311306-0118 N02/N03-W-353.2 ~J df-no2/no3 1 SEL Analrtes: N03N02N 1311306-011C 8260-W l'fl VOCFridge Test Group: 8260-W-Custom; #of Analytes: 4 I# ofSurr: 4 1311306-012A TW4-33_11142013 11/14/20 13 0849h 11/15/2013 0850h 300.0-W Aqueous I"'J df-wc 1 SEL Ant11yti.!S: CL 1311306-0128 N02/N03-W-353.2 v df-no2/no3 I SEL Analy tes: N03N02N Printed: 12/3/2013 WORK ORDER Summary Work Order: 1311306 Page 3 of3 Client: Energy Fuels Resources, Inc. Due Date: 11/26/2013 Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 1311306-012C TW4-33_11142013 11/14/2013 0849h 11115/2013 0850h 8260-W Aqueous ~I VOCFridge Test Group: 8260-W-Custom; #of Analytes: 4 I # ofSurr: 4 1311306-013A TW4-34_11142013 11/14/2013 0856h 11115/2013 0850h 300.0-W Aqueous IY'l df-wc 1 SEL Analytes: CL 1311306-0138 N02/N03-W-353.2 ~] df-no2/no3 1 SEL Analytes: N03N02N -----1311306-013C 8260-W l~i VOCFridge 3 Test Group: 8260-W-Custom; #of Analytes: 4 I # ofSurr: 4 1311306-0 14A TW4-60_11142013 11114/2013 0700h 11/1512013 0850h 300.0-W Aqueous ~I df-wc 1 SEL Analytes: CL 1311306-0148 N02/N03-W-353.2 !Jl df-no2/no3 1 SEL Ana lyles: N03N02N 1311306-014C 8260-W iV"I VOCFridge 3 Test Group: 8260-W-Custom; #of Ana lyles: 4 I # of Sun·: 4 1311306-015A TW4-l8R_lll22013 11112/2013 0827h 11115/2013 0850h 300.0-W Aqueous [~ df-wc 1 SEL Ana~V/e.t: CL 1311306-0158 N02/N03-W-353.2 fvl df-no2/no3 1 SEL Analytes: N03N02N 1311306-015C 8260-W [\(1 VOCFtidge 3 Test Group: 8260-W-Custom; #of Analytes: 4 I # ofSurr: 4 1311306-016A Trip Blank 11112/2013 11/15/2013 0850h 8260-W Aqueous I;( I VOCFridge j Test Group: 8260-W-Custom; #of Analytes: 4 I# of Surr: 4 Printed: 12/3/2013 AMERICAN WEST ANALYTICAL LABORATORIES 463 W, 3600 S. SALT LAKE CITY, UT 84n5 PHoNI! II (801) 263-8888 TOLL F'REE II (888) 263·8886 I ----·-·· ADDRESS: 6425 S. Hwy. 191 Blanding, UT 84511 CONTACT: Garrln Palmer PHONE#: (435) 678-2221 CELL#: gpalmo:r@cmOrgyfucla.com; KWch:tel@cmoruYfi:tela.cam; EMAIL: d~~fllo!s.=m PROJECT NAME: 4th Quarter Chloroform 2013 PROJECT#: PO#: SAMPLER NAME: Tanner Holliday DATE TIME SAMPLE ID: SAMPLED SAMPLED TW4-06_11132013 tl/13/ 1'3 700 TW4-05_11132013 !I/ 1:3) 13 708 TW4-18_11132013 ll/J!)/r~ 718 TW4-21_11132013 1\/1~/1.3 723 TW4-29_11132013 11/131/3 737 TW4-11_11132013 ll/1~/l:?> 745 TW4-07 _11142013 l\/i'-1/13 813 TW4-10_11142013 1{/!'{/l) 820 ~4-01_11142013 ll/ (1-\/l'\ 828 TW4-02_11142013 1\/['-\/5 833 TW4-32_11142013 H/11.\/i~ 842 TW4-33_11142013 ll/ 1'1(1) 849 TW4-34_11142013 llll"\/13 856 I CHAIN OF CUSTODY ALL ANALYSIS Wll..l.. Bl!!! CONDUCTeD USlNCI NELAP ACCRI!Dft'BD METHODS AND AU. DATA WILl.. ae R.BPORTED US:WG AWAL'& STANDARD ANALYTe U6TS AND RI!PORTI!'IQ UMrr.C (PQL) UNLZSS 3PEC:IPICALLY ReqUESTBO OTKBRWISII ON THlS CHAIN OF CUSTODY AND/OR ATTACHED DOCUMENTATiON QC LEVEL: I TURN AROUND TIME: UNLESS OTHER ARRANGIII:MEN1'S HAVE BEEN MADB, SIGNr:D RI!PQRTS WIU. 1!11! STANDARD EMAILBD BY 5:00 P~ ON THE tiAY 3 THEY ARe DUE. X INCLUDE EDD: LOCUS UPLOAD EXCEL FtELD FILTERED FoR: FOR COMPLIANCE WITH: 0 NELAP 0 RCRA 0 CWA 0 SDWA 0 ELAP I A2LA 0 NLLAP "' c;j' c 0 NoN-CoMPLIANCE It c:i Ill ~ ~ 0 OTHER: z Q ~ <'l D' ~ ~ ... ~ z (') 0 0 0 Q C'l u Ill 1!: ~ ~ KNOWN HAZARDS .J ll. ...... :t. " &. u. ~ N () 0 0 c:i 0 ,., Ill 12! > SAMPLE COMMENTS 5 w X X X s w X X X 5 ~ X X X " ~ X X X s ~ X X X 5 r.r X X X s " X X X s w X X X s ~ X X X 5 ~ X X X s ~ X X X s w X X X s ,. X X X REL.tt-.'QUIDltJI'Q BY: ---'1 II/// n11sJ~ =~~Q"h ~ / DATil: 1'/1'5'/o.~ SPECIAL INSTRUCTIONS: Sr<>NATURE ...-.. In iiA..O x ..,......, 6\rt,&r Hdll;cf{~ ~6'~ p,.?.d.~<-H.A-?t!"7 T"""r Y".f"rl PRINT NAME: 1311 '!Jo {p AWAL LAB SAMPLE SET'# PAGE 1 OF 2 ru•DA~ LABORATORY UsE ONLY SAMPLHS WER:<;:; 1 SKJPPBD 0 KA,.M~ O:;J • 2 AMSIE~:~ 3 Tl!MPI!RATURB °C 4 REC:BIVI!D BROKBN)'l...I!AKING (INPROPBRLY S0jo) y N ~O!'Im!:V PRESERV!!D y N tlota:D AT BI!NCH y N s Rec.eiVE.D WITHIN giNO TIMBS N CCC TAPII WM: 1 PRaseNT oN 0UTI!IR PAC:KA<II! y N ~ 2 UNBROK.N ON 0UTOr.:;JKACI• Y N NA \. 3 PRBSENT ON SAUPL. 8 Y N NA 4 UNOROKIIN ON SAMPEJ Y N NA 01SCAJ!PAHC~S BI!TW~BN SAMPLS l.AOO~ AND COC ~? ReLINQUISHED 15Y: ......_; DATE: ReceiVED BY: { DATI!!: See the Analytical Scope of Work for Reporting Limits and .SICiNATURE SI(JNATURE VOC analytc list. TlMI!!.: TIMS: PRINT NAMe: PRJNT NA.Me: ~UNQU~HZ!D BY: DATE: Recerveo ev: DATE: SIGNATURe SIGINATUAE TIME: iT"""' PRINT NAMJ!~ PRINT~ RI!UNQUlSHED BY: PATE' ftECEIVED BY: DATI!: SIGNATURE SIGNATURB TlME: TIME: PR!NJ" NA.M!!_;_ ~RlNT NAME: I AMERICAN WEST ANAL. YTICAL. LAB ORA TORIES CHAIN OF CUSTODY 463 W. 3600 S. SALT LAKE CITY. UT 84115 ALL ANALYSIS WILL BB CONDUCTI!ID USIN<J NELAP AC:::CAQDrT'E!D MI!THODS AND ALL DATA WILL BE RBPORTED USINI'3 AWAL1S STANDARD ANALYTE LISTS AND R!!POPtTINCJ UMrTS (PQL) UNLI!$S SPBCIPICAUY REQUI!!!STI!D OTHEA.WISB ON THIS PHONE# (801) 263-6686 TOLL FREE# (888) 263-6686 CHAIN OF CUSTCDY AHD/OR ATTACHI!D DOCUMBNTAT)ON I I QC LEVEL: I TURN AROUND TIME: UN..,.,. C>TliD!l AAJUU;Pil......,...ljAYa IJEIEIN MAD!!, SICJNBD RI!PoRTS WD.J.. De STANDARD I!MAJU!D I!SY 5:00 PM ON THE DAY 3 TH!!V ARI! DUe. --·-·-·· X INCLUDE EDD: 6425 S. Hwy. 191 LOCUS UPLOAD ADDRES-S; EXCEL Blanding, UT 84511 FIELD FILTERED FoR: - CONTACT: Garrin Palmer (435) 678-2221 FoR CoMPLIANce WITH: PHONE#: CELL#: 0 NELAP gpalmer@energyfu.eb;.com; KWeinel@energyfu.ela.com; 0 RCRA eMAIL: dmrk@!:ner&I!'!!;ela.com 0 CWA 4th Quarter Chloroform 2013 0 SDWA PROJECT NAME: I 0 ELAP I A2LA 0 NLLAP PROJECT#: Ill 0i' Ci' 0 NoN-CoMPLIANCE a: c:i w >< :;i 0 0 OTHER: PO#: z 0: "l li' ~ ~ (2 ... 0 Tanner Holliday z ::E 3 0 10 SAMPLER NAME: 0 0 ~ u w 0 ~ KNOWN HAZARDS ..J 2: li) • DATE TIME D. -::t. & ... ~ cot 0 0 0 f3 ~ SAMPLE! 10: SAMPLED SAMPLED • Ill 2: SAMPLE COMMENTS ~~_11142013 I l /1'1/!.) 700 5 w X X X TW4-18R_11122013 \1/ rz.J 13 827 5 w X X X TRIP BLANK ll/12./ 1:) 3 w X RmJNOUmtt~O BY~ jj~ S"'"ATURit -.. •ll tiJ1l/L o .. iJ!S/1:1 I . Race1va~~~ C1J S!tJN.O.TURA . ./ O.o.=.l//1~ k'7 SPECIAL INSTRUCTIONS: PR!NT NAtAe: --1'"' r.l'\c.-r Ho\\;~ T .. og~ !"BBNT NAM.{r I h-..t..... 4-/,J,_(L / 1'1MI!: rS"~ ~~ 11;~ G AWAL LAB SAMPLE SET# ---PAGE 2 OF 2 r••D•n' LABORATORY UsE ONLY SAMPLBS WI!RI!: 1 SHIPPeD CUI MA.ItD CIS Q 2 AMI!UI!NT C..IUl! 3 TKMPI!RATURE. ___:.t_ •c 4 RI!!CI!IYI!D BROKI!N/LIBAKING (IMPROPI!!RLY SBAU!D) y C) 5 c!}.""RLV PAeseRvoc y N C CKIID AT III!NCH y N 6 RBCEIVBD WrntlN IJ:;;LDIN<I T-.ces N coc TAP• Wid: 1 PReSENT ON OUTeR PAcKAoe y N ~ Y N /NA 2 UNBROKEN ON 0UT(:3CKAG2 3 PRESINT ON SAMPL.a 8 Y N NA 4 UNOROK.N ON S.O.MP~ Y N NA Ol=C1UtJ•AMC:.mi: BBTWI!I!N SAMPU! y N IJ.JI .... AND coc ORD? RllutaUC'Hl!O ev: _; o ... ,.., 'R.I!!CBJVI!D BY: t / DATI!: See the Analytical Scope of Work for Reporting Limits and Sk!NATURD SIGNATURE VOC analyte list. TIMe: TIMe: p,.....,~ PRJN't NAMI!: Rr.:LINQUISHE!D BY: DATI!: RIC:IUYlr-0 • .,.: DATE: SI<JNATUR..I!!! $~,4-Aj!'UAW T'ME! T»Ae: PRJNT NAMe: PRrtn NAME!: ~E!UNQU&SH!!D BY: DATil: RecaJVBD ev: DATE: SIGNATURe SICJNATURI! TIM I!: ·-PRINT NAME!': -~ J0ot"'" NAMI!J_ I I I I A W AL -Analytical Scope of Work White Mesa Mill Blanding Utah Page 11 of 13 Sulfate ~r-r-IDg/L 2~ None -----E300.0 r r------_ Carbona~03 A2320 B 1 mg/L 14 days None ~ ~bqnatc as HC03 A2320 B 1 mg/L 14 days None ---._ nrat}te;djigaJXir-%mn:oJmos~J'lfOi:~fQib:i'{Pfqgr:Wn~ "'"' ~ . ';' ~~@~:.-·. ~ .-·"-~:;.,. ~.' Carbon Tetrachloride SW8260B 1.0 ~giL 14 days HCl to pH<2 :::; 6°C Chloroform Dichloromethane (Methylene Chloride) Chloromethane or SW8260C SW8260B or SW8260C SW8260B or SW8260C SW8260B or SW8260C l.O~g!L 14 days HCl to pH<2 :S::6°C 1.0 ~giL 14 days HCl topH<2 :::; 6°C l.OJlg/L 14 days HCl to pH<2 :S::6°C ff:\(.oes::.:':f~llh,~irw.powllithenf'S~pJes ®litY.":. · .~ ~-;. ~ :' •.· ~-.., .t···..,.:~~:., ~ _ =-~ . ..A 1 2,4'*icli.lorobenzene SW8270D <10 ug!L 7/40 days None <JYC 1,2-Dichl~enzene SW8270D <10 ug!L 7/40 days None A 6°C 1,_,3-Dicblorob-ue. SW8270D <10 ug!L 7/40 days None ......_./ < 6°C 1,4-Dichlorobeozene--....,. SW8270D <10 u_,g!L 7/40 days Non~ .::::. 6°C 1-Methylnapbthalene ~ SW8270D <10 ug!L 7/40 days ..,N6ne < 6°C 2;4,5-Trichlorophenol ~8270D <10 ug!L 7/40 days V None < 6°C .2,4,6-Trichlorophe.aol SW~D <10 ug/L 7/40 da~ None < 6°C 2.4~Dichlorophenol SW8270.0'-<10 ug!L 7/4,011'ays None < 6°C 2,4-Di.m.eth.ylphenol SW8270D <~giL ~40 days None < 6°C 2,4-Dinitrop11enol SW8270D <20 u~ 7/40 days None :::: 6°C 2,4-Dinitrotoluene SW8270D ~giL ~40 days None :::::; 6°C 2,6-Dinitrotoluene SW8270D/v<10 ug/L 7/41N4!Js None :::: 6°C 2-CWOl'onaphtbalene SW~D <10 ug!L 7/40 da~ None < 6°C 2-ChloroQhenol ~8270D <1 0 ug!L 7/40 days ~ None < 6°C 2-Methylnaphthalenc ./ SW8270D <10 ug!L 7/40 days l'fst:le :S6°C 2-Methylphenol / SW8270D <10 ug/L 7/40 days Non~ < 6°C 2-Nio:ophenoJ ~ SW8270D <10 ug/l 7/40 days None ........_ < 6°C 3&4-Meth~enol SW8270D <10 ug!L 7/40 days None ~6°C 3,3 '-:p.iclilorobenzidine SW8270D <10 ug!L 7/40 days None < 6"'&.. 4)(-Dinitro-2-methylphenol SW8270D <1 0 ug!L 7/40 days None :S 6°C ........._ Analysis Ammonia COD Cyanide Metals NOa&NOs" O&G Phenols Sulfide TKN TP04 Procedure: Frequency: Preservation Check Sheet s le Set E Preservative I 2.. ~ '( ') ~ pH<Z H2S04 pH<2 H2SO<~- pH>12 NaOH pK<2 HNO; PH <2 H2S04 V'c:-J VeS" tle:_s .Vcs !kf YeS pH <2HCL I' I I' pH <ZH2S04 pH>9NaOH, Zn Acetate pH <2H2S04 pH <Z H2SQ4 - ----- Pour a small amount of sample in the sample lid Pour samp_le from Lid genU_y over wide range pH paper Do N"ot dip tbe pH paper in the sample bottle or lid 7 ya; I/ dDH 7 ( Yes v6 /(l !I YC"S" ~~ 17 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * The sample required additional preservative upon receipt. + The sample was received unpreserved • The Sample was received unpreserved and therefore preserved upon receipt. # The sample pH was unadjustable to a pH < 2 due to the sample matrix • The sample pH was unadjustable to a pH > __ due to the sample matrix interference Lab SetiD: / {;; / /)0 fJ /z.-. I} ;-( ;;J rh Yc:> fk.r v't7 7 ~- TabH Quality Assurance and Data Validation Tables H-1 Field Data QAJQC Evaluation Voltime L<roation 2x Caslng Volume Pu~p~ Volume Cheek Piezometer 1 - Piezometer 2 -- Piezometer 3 -- TWN-1 36.30 72.60 88.00 OK TWN-2 NA Cont inuousLy Pum_ped Well TWN-3 38.39 76.78 52.00 Pumped Dry TWN-4 50.07 100.14 121.00 OK TWN-7 11.81 23.62 19.00 Pumped Dry_ TWN-18 56.29 112.58 132.00 OK TW4-22 NA Comlnu_ously pumped well TW4-24 NA Continuously pumpc~d well TW4-25 NA O.munupusly pumped well NC = Not Calculated TWN-2, TW4-22, TW4-24, and TW4-25 are continuously pumping wells. Piezometers I, 2, and 3 were not pumped, only one set of parameters were taken. TWN-3 and TWN-7 were pumped dry and sampled after recovery. Conduttivity RPD 2175 NC 701 NC 2943 NC 854.0 856.0 0.23 7.20 3578 NC 2485.0 2476.0 0.36 7.22 1056.0 1057.0 0.09 7.18 1194.0 1200.0 0.50 7.14 2210.0 2218.0 0.36 6.85 6383 NC 8024 NC 2759 NC PH RED Temp RPD Red8x Potential RPD Turbiaity RPD 8.73 NC 13.40 NC 327 NC 9.0 NC 7.45 NC 13.47 NC 290 NC 6.5 NC 11.60 NC 13.51 NC 237 NC 9.6 NC 7.26 0.83 14.61 14.68 0.48 335 I 330 1.50 56 I 59 5.22 6.63 NC 13.51 NC 320 NC 0 NC 7.19 0.42 14.50 14.47 0.21 NM NC NM NC 7.18 0.00 14.44 14.44 0.00 296 I 292 1.36 316.0 1 325.0 2.81 7.12 0.28 14.29 14.31 0.14 NM NC NM NC 6.85 0.00 14.36 14.40 0.28 299 I 299 0.00 1048.o I 1059.0 1.04 6.93 NC 15.41 NC 242 NC 0 NC 6.85 NC 15.11 NC 250 NC 0 NC 7.09 NC 16.55 NC 269 NC 0 NC The QAP states that turbidity should be less than 5 Nephelometric Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measLirements less than 5 NTU below are included for information purposes only. NM =Not Measured. The QAP does not require the measurement of redox potential or turbidity in wells that were purged to dryness. H-2: Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check PIEZ-01 Chloride 10116/2013 10/21/2013 5 28 OK PIEZ-01 Nitrate/Nitrite (as N) 10/16/2013 10/22/2013 6 28 OK PIEZ-02 Chloride 10/16/2013 10/22/2013 6 28 OK PIEZ-02 Nitrate/Nitrite (as N) 10/16/2013 10/22/2013 6 28 OK PIEZ-03 Chloride 10/16/2013 10122/2013 6 28 OK PIEZ-03 Nitrate/Nitrite (as N) 10/16/2013 10/22/2013 6 28 OK TWN-01 Chloride 10/16/2013 10/21/2013 5 28 OK TWN-01 Nitrate/Nitrite (as N) 10116/2013 10/22/2013 6 28 OK TWN-02 Chloride 10/16/2013 10/21/2013 5 28 OK TWN-02 Nitrate/Nitrite (as N) 10/16/2013 10/22/2013 6 28 OK TWN-03 Chloride 10/17/2013 10/21/2013 4 28 OK TWN-03 Nitrate/Nitrite (as N) 10117/2013 10/22/2013 5 28 OK TWN-04 Chloride 10116/2013 10/21/2013 5 28 OK TWN-04 Nitrate/Nitrite (as N) 10116/2013 10/2212013 6 28 OK TWN-07 Chloride 10/16/2013 10/21/2013 5 28 OK TWN-07 Nitrate/Nitrite (as N) 10/16/2013 10/22/2013 6 28 OK TWN-07R Chloride 10115/2013 10/21/2013 6 28 OK TWN-07R Nitrate/Nitrite (as N) 10115/2013 10/22/2013 7 28 OK TWN-18 Chloride 10/16/2013 10/21/2013 5 28 OK TWN-18 Nitrate/Nitrite (as N) 10116/2013 10/22/2013 6 28 OK TW4-22 Chloride 10/29/2013 1113/2013 5 28 OK TW4-22 Nitrate/Nitrite (as N) 10/29/2013 11/5/2013 7 28 OK TW4-24 Chloride 10/29/2013 1113/2013 5 28 OK TW4-24 Nitrate/Nitrite (as N) 10/29/2013 11/5/2013 7 28 OK TW4-25 Chloride 10/29/2013 11/3/2013 5 28 OK TW4-25 Nitrate/Nitrite (as N) 10/29/2013 11/5/2013 7 28 OK TW4-60 Chloride 11114/2013 11/22/2013 8 28 OK TW4-60 Nitrate/Nitrite (as N) 11/14/2013 11/15/2013 1 28 OK TWN-60 Chloride 10/17/2013 10/21/2013 4 28 OK TWN-60 Nitrate/Nitrite (as N) 10/17/2013 10/22/2013 5 28 OK TWN-65 Chloride 10/16/2013 10/21/2013 5 28 OK TWN-65 Nitrate/Nitrite (as N) 10/16/2013 10/22/2013 6 28 OK H-3: Analytical Method Check "Par~ Method Method Ufwd by Lab Nitrate E353.1 or E353 .2 E353.2 A4500-CI B or A4500-CI E Chloride or£300.0 E300.0 Both Nitrate and Chloride were analyzed with the correct analytical method. -cportm~ JIDJt ec H 4 R L' . Ch k Required 111 Lab Reporting Reporting Location ·AnlllyJ,c Limit Units Qualifier Limit Units RLCheck PIEZ-01 Chloride 10 mg!L 1 mg/L OK PIEZ-01 Nitrate/Nitrite (as N) I mg/L O.I mg!L OK PIEZ-02 Chloride 5 mg!L I mg!l OK PIEZ-02 Nitrate/Nitrite (as N) O.I mg/L O.I mg!L OK PIEZ-03 Chloride 5 mg/L 1 mg!L OK PIEZ-03 Nitrate/Nitrite (as N) 0.1 mg/L O.I mg!L OK TWN-OI Chloride 5 mg!L 1 mg/L OK TWN-OI Nitrate/Nitrite (as N) 0.5 mg!L 0.1 mg/L OK TWN-02 Chloride 10 mg!L 1 mg/L OK TWN-02 Nitrate/Nitrite (as N) 10 mg!L O.I mg!L OK TWN-03 Chloride 50 mg/L 1 mg!L OK TWN-03 Nitrate/Nitrite (as N) 2 mg/L 0.1 mg!L OK TWN-04 Chloride 5 mg!L 1 m_g!L OK TWN-04 Nitrate/Nitrite (as N) 0.5 mg!L 0.1 mg/L OK TWN-07 Chloride I mg!L 1 mg!L OK TWN-07 Nitrate/Nitrite (as N) 0.1 mg!L O.I mg_IL OK TWN-07R Chloride I mg_IL u 1 mg!L OK TWN-07R Nitrate/Nitrite (as N) 0.1 mg/L u 0.1 mg/L OK TWN-18 Chloride 10 mg!L 1 mg/L OK TWN-18 Nitrate/Nitrite (as N) 0.5 mg!L 0.1 mg!L OK TW4-22 Chloride 100 mg!L 1 mg/L OK TW4-22 Nitrate/Nitrite (as N) 10 mg!L 0.1 mg/L OK TW4-24 Chloride 100 mg/L 1 mg/L OK TW4-24 Nitrate/Nitrite (as N) 10 mg!L 0.1 mg!L OK TW4-25 Chloride 50 mg/L 1 mg!L OK TW4-25 Nitrate/Nitrite (as N) 1 mg/L 0.1 mg!L OK TW4-60 Chloride I mg/L u 1 mg!L OK TW4-60 Nitrate/Nitrite (as N) 0.1 mg!L u O.I mg/L OK TWN-60 Chloride 1 mg/L u 1 mg!L OK TWN-60 Nitrate/Nitrite (as N) 0.1 mg/L u 0.1 mg!L OK TWN-65 Chloride 5 mg/L 1 mg!L OK TWN-65 Nitrate/Nitrite (as N) O.I mt:ll O.I mg!L OK U = Value was reported by the laboratory as nondetect. H-5 QA/QC Evaluation for Sample Duplicates CoJ\Stituent 'fWNo(Jl TWN-6.5 %'RPD Chloride 28.6 27.1 5.39 Nitrogen 1.61 1.48 8.41 H-6 QC Control Limits for Analysis and Blanks Method Blank Detections All Method Blanks for the quarter were non-detect. Matrix Soike% Recovcrv C -~·-· ------- REC Lab Report Lab Sample ID Well Analyte MS %REC MSD%REC Range RPD 1311306 1311306-001BMS TW4-06 Nitrate 89.2 97.6 90-110 10.4 1311306 1311306-007BMS TW4-07 Nitrate 113 110 90-110 15.4 Laboratory Control Sample All Laboratory Control Samples were within acceptance limits for the quarter. . T H-7 Hcc-cipl ¢mperarure EvaluatiOn Saml)le Batilh Well$; h-. Dafc.1h Tfln»eral'lire 1310396 Piezometer 1, Piezometer 2, Piezometer 3, TWN-1, TWN-2, 1.4°C TWN-3, TWN-4, TWN-7, TWN-18, TWN-60, TWN-65 1310621 TW4-22, TW4-24. TW4-25 0.9 oc 1311306 TW4-60 4.8 oc H-8 Rinsate Evaluation All Rinsate and DI Blank samples were non-detect for the quarter. Tab I Kriged Current Quarter Isoconcentration Maps NS =not sampled; ND =not detected ......_10 MW-4 e s.3 TW4-1 0 7.1 TWN-1 ¢1.6 PIEZ-1 Q 6.7 TW4-32 ~4.3 kriged nitrate isocon and label perched monitoring well showing concentration in mg/L temporary perched monitoring well showing concentration in mg/L temporary perched nitrate monitoring well showing concentration in mg/L perched piezometer showing concentration in mg/L temporary perched monitoring well installed September, 2013 showing concentration in mg/L NOTE: MW-4, MW-26, TW4-4, TW4-19, and TW4-20 are chloroform pumping wells; TW4-22, TW4-24, TW4-25, and TWN-2 are nitrate pumping wells HYDRO GEO CHEM,INC. KRIGED 4th QUARTER, 2013 NITRATE (mg/L) (NITRATE + NITRITE AS N) WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H:/718000/feb14/nitrate/Unt1213.srf I I -1 NS = not sampled; ND = not detected ......_ 100 ktiged chloride isooon ar:~d label MW-4 .40 TW4-1 0 37 TWN-1 ~27 PIEZ-1 g 54 TW4-32 ~52 perched monitoring well showing concentration in mg/L temporary perched monitoring well showing concentration in mg/L temporary perched nitrate monitoring well showing concentration in mg/L perched piezometer showing concentration in mg/L temporary perched monitoring well installed September, 2013 showing concentration in mg/L NOTE: MW-4, MW-26, TW4-4, TW4-19, and TW4-20 are chloroform pumping wells; TW4-22, TW4-24, TW4-25, and TWN-2 are nitrate pumping wells HYDRO GEO CHEM,INC. KRIGED 4th QUARTER, 2013 CHLORIDE (mg/L) WHITE MESA SITE APPROVED DATE fii:Ff;RENCE I FIGURE H:/718000/feb14/chloride/Ucl1213.srf I-2 TabJ Analyte Concentrations Over Time Piezometer 1 Date Nitrate (mg/1) Chloride (mg/1) 2/19/2009 6.8 NA 7/14/2009 6.8 60 9/22/2009 7.3 78 10/27/2009 7.4 61 6/2/2010 7.2 52 7/19/2010 6.8 52 12/10/2010 6.5 60 1/31/2011 7 60 4/25/2011 6.8 58 7/25/2011 7 53 10/19/2011 6.6 55 1/11/2012 7.1 78 4/20/2012 6.6 58 7/27/2012 7.2 56 10/17/2012 7.66 55 2/18/2013 8.11 56.7 4/24/2013 8.88 53.3 8/28/2013 7.83 55.1 10/16/2013 6.68 54.1 Piezometer 2 Date Nitrate (mg/1) Chloride (mg/1) 2/19/2009 0.5 NA 7/14/2009 0.5 7 9/22/2009 0.5 17 10/27/2009 0.6 7 6/2/2010 0.6 8 7/19/2010 0.6 8 12/10/2010 0.2 6 1/31/2011 0.3 9 4/25/2011 0.3 8 7/25/2011 0.1 9 10/19/2011 0.1 8 1/11/2012 0.1 9 4/20/2012 0.2 8 7/27/2012 0.2 9 10/17/2012 0.192 9.5 2/19/2013 0.218 9.67 4/24/2013 0.172 10.3 8/28/2013 0.198 9.66 10/16/2013 0.364 9.22 Piezometer 3 Date Nitrate (mg/1) Chloride (mg/1) 2/19/2009 0.7 NA 7/14/2009 0.8 12 9/22/2009 0.8 24 10/27/2009 1.2 19 3/24/2010 1.7 116 6/2/2010 1.6 36 7/19/2010 1.6 35 12/10/2010 1.8 25 1/31/2011 1.8 40 4/25/2011 1.7 35 7/25/2011 1.8 61 10/19/2011 1.7 12 1/11/2012 1.8 20 4/20/2012 1.7 53 7/27/2012 1.8 21 10/17/2012 2.75 20.1 2/19/2013 1.85 21 4/24/2013 1.83 21.2 8/28/2013 1.81 22.4 10/16/2013 1.80 23.5 TWN-1 Date Nitrate (mg/1) Chloride (mg/1) 2/6/2009 0.7 19 7/21/2009 0.4 17 9/21/2009 0.4 19 10/28/2009 0.5 18 3/17/2010 0.5 17 5/26/2010 0.6 20 9/27/2010 0.6 19 12/7/2010 0.6 14 1/26/2011 0.5 17 4/20/2011 0.5 19 7/26/2011 0.5 14 10/17/2011 0.5 10 1/9/2012 0.6 15 4/18/2012 0.6 17 7/24/2012 0.6 17 10/15/2012 0.432 17.5 2/18/2013 0.681 17.6 4/23/2013 0.84 17.4 8/27/2013 1.24 24.1 10/16/2013 1.61 26.8 TWN-2 Date Nitrate (mg/1) Chloride (mg/1) 2/6/2009 25.4 29 7/21/2009 25 25 9/21/2009 22.6 17 11/2/2009 20.8 55 3/24/2010 62.1 85 6/2/2010 69 97 9/29/2010 69 104 12/9/2010 48 93 2/1/2011 43 93 4/28/2011 40 85 7/28/2011 33 74 10/20/2011 33 76 1/12/2012 31 86 4/20/2012 48 103 7/31/2012 54 93 10/17/2012 22.1 79 2/19/2013 57.3 80.5 4/24/2013 57.7 82.1 8/27/2013 80 75.9 10/16/2013 111 70.4 TWN-3 Date Nitrate (mg/1) Chloride (mg/1) 2/6/2009 23.6 96 7/21/2009 25.3 96 9/21/2009 27.1 99 11/2/2009 29 106 3/25/2010 25.3 111 6/3/2010 26 118 7/15/2010 27 106 12/10/2010 24 117 2/1/2011 24 138 4/28/2011 26 128 7/29/2011 25 134 10/20/2011 25 129 1/12/2012 25 143 4/20/2012 24 152 7/31/2012 27 158 10/17/2012 12.1 149 2/19/2013 22.2 157 4/24/2013 27.2 158 8/28/2013 20.9 171 10/17/2013 23.5 163 TWN-4 Date Nitrate (mg/1) Chloride (mg/1) 2/6/2009 1 13 7/21/2009 0.05 12 9/21/2009 0.4 13 10/28/2009 0.4 11 3/16/2010 0.9 22 5/27/2010 1.0 22 9/27/2010 0.9 19 12/8/2010 1 21 1/25/2011 0.9 21 4/20/2011 0.9 21 7/26/2011 1.1 35 10/18/2011 0.9 20 1/9/2012 0.9 20 4/18/2012 1.1 24 7/25/2012 1.4 25 10/15/2012 1.45 26.4 2/18/2013 1.51 25.3 4/23/2013 1.63 24.4 8/27/2013 1.58 27.2 10/16/2013 1.69 29.4 TWN-7 Date Nitrate (mg/1) Chloride (mg/1) 8/25/2009 ND 11 9/21/2009 ND 7 11/10/2009 0.1 7 3/17/2010 0.8 6 5/28/2010 1.2 6 7/14/2010 1.6 7 12/10/2010 1 4 1/27/2011 1.3 6 4/21/2011 1.7 6 7/29/2011 0.7 5 10/19/2011 2.2 6 1/11/2012 2.3 5 4/20/2012 1.2 6 7/26/2012 0.9 6 10/16/2012 0.641 5.67 2/19/2013 0.591 5.68 4/24/2013 1.16 5.88 8/28/2013 0.835 6.96 10/16/2013 0.986 5.70 TWN-18 Date Nitrate (mg/1) Chloride (mg/1) 11/2/2009 1.3 57 3/17/2010 1.6 42 6/1/2010 1.8 63 9/27/2010 1.8 64 12/9/2010 1.6 59 1/27/2011 1.4 61 4/26/2011 1.8 67 7/28/2011 1.8 65 10/18/2011 1.9 60 1/10/2012 1.9 64 4/19/2012 2.1 64 7/26/2012 2.3 67 10/16/2012 1.95 67.5 2/18/2013 2.27 68.7 4/23/2013 2.32 64.3 8/27/2013 2.04 70.4 10/16/2013 2.15 67.3 TW4-19 Date Nitrate (mg/1) Date Chloride (mg/1) 7/22/2002 42.80 12/7/2005 81 9/12/2002 47.60 3/9/2006 86 3/28/2003 61.40 7/20/2006 123 6/23/2003 11.40 11/9/2006 134 7/15/2003 6.80 2/28/2007 133 8/15/2003 4.00 8/15/2007 129 9/12/2003 5.70 10/10/2007 132 9/25/2003 9.20 3/26/2008 131 10/29/2003 7.70 6/25/2008 128 11/9/2003 4.80 9/10/2008 113 8/16/2004 9.91 10/15/2008 124 9/17/2004 4.50 3/4/2009 127 3/16/2005 5.30 6/23/2009 132 6/7/2005 5.70 9/14/2009 43 8/31/2005 4.60 12/14/2009 124 12/1/2005 0.10 2/17/2010 144 3/9/2006 4.00 6/9/2010 132 6/14/2006 5.20 8/16/2010 142 7/20/2006 4.30 10/11/2010 146 11/9/2006 4.60 2/17/2011 135 2/28/2007 4.00 6/7/2011 148 8/15/2007 4.10 8/17/2011 148 10/10/2007 4.00 11/17/2011 148 3/26/2008 2.20 1/23/2012 138 6/25/2008 2.81 6/6/2012 149 9/10/2008 36.20 9/5/2012 149 10/15/2008 47.80 10/3/2012 150 3/4/2009 3.20 2/11/2013 164 6/23/2009 2.40 6/5/2013 148 9/14/2009 0.10 9/3/2013 179 12/14/2009 26.70 10/29/2013 206 2/17/2010 2.00 6/9/2010 4.40 8/16/2010 5.90 10/11/2010 2.70 2/17/2011 17.00 6/7/2011 12.00 8/17/2011 3.00 11/17/2011 5.00 1/23/2012 0.60 6/6/2012 2.40 9/5/2012 2.50 10/3/2012 4.10 2/11/2013 7.99 6/5/2013 2.95 9/3/2013 17.60 10/29/2013 4.70 The sampling program for TW4-19 was updated in the fourth quarter of 2005 to include analysis for chloride as well as nitrate. This change accounts for the different number of data points represented above. TW4-21 Date Nitrate (mg/1) Date Chloride (mg/1) 5/25/2005 14.6 12/7/2005 353 8/31/2005 10.1 3/9/2006 347 11/30/2005 9.6 7/20/2006 357 3/9/2006 8.5 11/8/2006 296 6/14/2006 10.2 2/28/2007 306 7/20/2006 8.9 6/27/2007 327 11/8/2006 8.7 8/15/2007 300 2/28/2007 8.7 10/10/2007 288 6/27/2007 8.6 3/26/2008 331 8/15/2007 8.6 6/25/2008 271 10/10/2007 8.3 9/10/2008 244 3/26/2008 14.3 10/15/2008 284 6/25/2008 8.8 3/11/2009 279 9/10/2008 7.6 6/24/2009 291 10/15/2008 8.0 9/15/2009 281 3/11/2009 8.3 12/22/2009 256 6/24/2009 8.1 2/25/2010 228 9/15/2009 9.2 6/10/2010 266 12/22/2009 8.4 8/12/2010 278 2/25/2010 8.4 10/13/2010 210 6/10/2010 12.0 2/22/2011 303 8/12/2010 14.0 6/1/2011 297 10/13/2010 7.0 8/17/2011 287 2/22/2011 9.0 11/16/2011 276 6/1/2011 13.0 1/19/2012 228 8/17/2011 14.0 6/13/2012 285 11/16/2011 13.0 9/13/2012 142 1/19/2012 15.0 10/4/2012 270 6/13/2012 11.0 2/13/2013 221 9/13/2012 13.0 6/18/2013 243 10/4/2012 14.0 9/12/2013 207 2/13/2013 11.8 11/13/2013 206 6/18/2013 13.8 9/12/2013 10.3 11/13/2013 9.0 The sampling program for TW4-21 was updated in the fourth quarter of 2005 to include analysis for chloride as well as nitrate. This change accounts for the different number of data points represented above. TW4-22 Date Nitrate (mg/1) Chloride (mg/1) 2/28/2007 20.9 347 6/27/2007 19.3 273 8/15/2007 19.3 259 10/10/2007 18.8 238 3/26/2008 39.1 519 6/25/2008 41.9 271 9/10/2008 38.7 524 10/15/2008 36.3 539 3/11/2009 20.7 177 6/24/2009 20.6 177 9/15/2009 40.3 391 12/29/2009 17.8 175 3/3/2010 36.6 427 6/15/2010 19 134 8/12/2010 18 127 8/24/2010 15 130 10/13/2010 16 134 2/23/2011 18 114 6/1/2011 17 138 8/17/2011 15 120 11/16/2011 19 174 1/19/2012 14 36 6/13/2012 12.8 35 9/12/2012 7 121 10/4/2012 14 130 2/11/2013 58 635 6/5/2013 50.2 586 9/3/2013 29.7 487 10/29/2013 45.2 501 TW4-24 Date Nitrate (mg/1) Chloride (mg/1) 6/27/2007 26.1 770 8/15/2007 29 791 10/10/2007 24.7 692 3/26/2008 24.4 740 6/25/2008 45.3 834 9/10/2008 38.4 1180 10/15/2008 44.6 1130 3/4/2009 30.5 1010 6/24/2009 30.4 759 9/15/2009 30.7 618 12/17/2009 28.3 1080 2/25/2010 33.1 896 6/9/2010 30 639 8/11/2010 32 556 8/24/2010 31 587 10/6/2010 31 522 2/17/2011 31 1100 5/26/2011 35 1110 8/17/2011 34 967 11/16/2011 35 608 1/18/2012 37 373 6/6/2012 37 355 8/30/2012 37 489 10/3/2012 38 405 2/11/2013 35.9 1260 6/5/2013 23.7 916 9/3/2013 32.6 998 10/29/2013 34.6 1030 TW4-25 Date Nitrate (mg/1) Chloride (mg/1) Notes 6/27/2007 17.1 395 8/15/2007 16.7 382 10/10/2007 17 356 3/26/2008 18.7 374 6/25/2008 22.1 344 9/10/2008 18.8 333 10/15/2008 21.3 366 3/4/2009 15.3 332 6/24/2009 15.3 328 9/15/2009 3.3 328 12/16/2009 14.2 371 2/23/2010 14.4 296 6/8/2010 16 306 8/10/2010 14 250 10/5/2010 15 312 2/16/2011 15 315 5/25/2011 16 321 8/16/2011 16 276 11/15/2011 16 294 1/18/2012 16 304 5/31/2012 16 287 9/11/2012 17 334 10/3/2012 17 338 2/11/2013 9.04 190 6/5/2013 5.24 136 9/3/2013 5.69 119 10/29/2013 6.10 88.6 MW-30 Date Nitrate (mg/1) Date Chloride (mg/1) 6/22/2005 12.4 6/22/2005 125 9/22/2005 12.8 9/22/2005 125 12/14/2005 13.6 12/14/2005 128 3/22/2006 13.8 3/22/2006 125 6/21/2006 14.5 6/21/2006 124 9/13/2006 14.1 9/13/2006 118 10/25/2006 14.6 10/25/2006 124 3/15/2007 14.4 3/15/2007 125 8/22/2007 14.6 8/22/2007 126 10/24/2007 14.9 10/24/2007 122 3/19/2008 14.8 3/19/2008 118 6/3/2008 18.7 6/3/2008 125 8/4/2008 17.3 8/4/2008 121 11/5/2008 15.6 11/5/2008 162 2/3/2009 15.3 2/3/2009 113 5/13/2009 15.1 5/13/2009 122 8/24/2009 20.9 8/24/2009 118 10/14/2009 15.0 10/14/2009 129 1/20/2010 15.4 1/20/2010 106 2/9/2010 16.1 2/9/2010 127 4/27/2010 15.8 4/27/2010 97 5/24/2010 17.0 9/14/2010 111 6/15/2010 15.3 11/9/2010 126 8/24/2010 16.0 2/1/2011 134 9/14/2010 15.0 4/11/2011 134 10/19/2010 15.0 5/10/2011 128 11/9/2010 15.0 6/20/2011 127 12/14/2010 16.0 7/5/2011 127 1/10/2011 15.0 8/3/2011 126 2/1/2011 16.0 9/7/2011 145 3/14/2011 17.0 10/4/2011 129 4/11/2011 16.0 11/8/2011 122 5/10/2011 16.0 12/12/2011 124 6/20/2011 17.0 1/24/2012 124 7/5/2011 17.0 2/14/2012 126 8/3/2011 14.0 3/14/2012 128 9/7/2011 16.0 4/10/2012 128 10/4/2011 16.0 5/2/2012 124 11/8/2011 16.0 6/18/2012 131 12/12/2011 16.0 7/10/2012 128 1/24/2012 17.0 8/7/2012 139 2/14/2012 17.0 9/19/2012 130 3/14/2012 18.0 10/23/2012 135 4/10/2012 17.0 11/13/2012 114 5/2/2012 16.0 12/26/2012 122 MW-30 Date Nitrate (mg/1) Date Chloride (mg/1) 6/18/2012 15.0 1/23/2013 128 7/10/2012 17.0 2/26/2013 129 8/7/2012 18.0 3/20/2013 126 9/19/2012 16.0 4/17/2013 117 10/23/2012 16.2 5/15/2013 119 11/13/2012 18.5 6/25/2013 127 12/26/2012 17.2 7/10/2013 130 1/23/2013 19.2 8/20/2013 126 2/26/2013 21.4 9/18/2013 131 3/20/2013 14.3 10/22/2013 128 4/17/2013 16.8 11/20/2013 124 5/15/2013 18.8 12/18/2013 134 6/25/2013 16.1 7/10/2013 17.6 8/20/2013 16.4 9/18/2013 16.9 10/22/2013 19.7 11/20/2013 19.5 12/18/2013 20.7 Under the groundwater sampling progran, accelerated monitoring for nitrate began in MW- 30 prior to when the accelerated monitoring for chloride began . This difference accounts for the different number of data points represented above. MW-31 Date Nitrate (mg/1) Date Chloride (mg/1) 6/22/2005 24.2 6/22/2005 139 9/22/2005 22.4 9/22/2005 136 12/14/2005 23.8 12/14/2005 135 3/22/2006 24.1 3/22/2006 133 6/21/2006 25.3 6/21/2006 138 9/13/2006 24.6 9/13/2006 131 10/25/2006 25.1 10/25/2006 127 3/15/2007 23.2 3/15/2007 132 3/15/2007 22.0 3/15/2007 132 8/27/2007 23.3 8/27/2007 136 10/24/2007 24.6 10/24/2007 122 3/19/2008 25.0 3/19/2008 124 6/3/2008 29.3 6/3/2008 128 8/4/2008 28.7 8/4/2008 124 11/11/2008 29.9 11/11/2008 119 2/3/2009 23.4 2/3/2009 115 5/13/2009 22.4 5/13/2009 124 8/24/2009 15.4 8/24/2009 122 10/14/2009 22.6 10/14/2009 138 2/9/2010 21.7 2/9/2010 128 4/20/2010 22.5 4/20/2010 128 5/21/2010 23.0 9/13/2010 139 6/15/2010 21.1 11/9/2010 138 8/24/2010 22.0 2/1/2011 145 9/13/2010 21.0 4/1/2011 143 10/19/2010 20.0 5/10/2011 143 11/9/2010 20.0 6/20/2011 145 12/14/2010 20.0 7/5/2011 148 1/10/2011 19.0 8/2/2011 148 2/1/2011 21.0 9/6/2011 148 3/14/2011 22.0 10/3/2011 145 4/1/2011 21.0 11/8/2011 145 5/10/2011 20.0 12/12/2011 148 6/20/2011 22.0 1/24/2012 155 7/5/2011 22.0 2/13/2012 150 8/2/2011 20.0 3/13/2012 152 9/6/2011 21.0 4/9/2012 160 10/3/2011 21.0 5/2/2012 151 11/8/2011 21.0 6/18/2012 138 12/12/2011 21.0 7/9/2012 161 1/24/2012 21.0 8/6/2012 175 2/13/2012 21.0 9/18/2012 172 3/13/2012 22.0 10/22/2012 157 4/9/2012 21.0 11/6/2012 189 5/2/2012 20.0 12/18/2012 170 MW-31 Date Nitrate (mg/1) Date Chloride (mg/1) 6/18/2012 21.6 1/22/2013 176 7/9/2012 21.0 2/19/2013 174 8/6/2012 21.0 3/19/2013 168 9/18/2012 21.0 4/16/2013 171 10/22/2012 18.0 5/13/2013 169 11/6/2012 23.6 6/24/2013 179 12/18/2012 22.2 7/9/2013 182 1/22/2013 22.8 8/19/2013 183 2/19/2013 19.3 9/17/2013 193 3/19/2013 19.1 10/23/2013 188 4/16/2013 18.8 11/18/2013 174 5/13/2013 23.8 12/17/2013 203 6/24/2013 20.0 7/9/2013 21.7 8/19/2013 16.0 9/17/2013 21.2 10/23/2013 21.2 11/18/2013 23.9 12/17/2013 24.2 Under the groundwater sampling progran, accelerated monitoring for nitrate began in MW-31 prior to when the accelerated monitoring for chloride began. This difference accounts for the different number of data points represented above. TabK Concentration Trend Graphs 1/) ~ 0 --; 1lo. -~ Q) u ~ 0 0 .! ca 1lo. .t: z "'"" 1lo. Q) a; E 0 .~ c.. < 0 ,.- ~ ~ ! 1\ > 4 > ~ ~ ~ , ~, ' ~ v~-unr . 8~-AON 8 ~ -liBV\1 ~~-des o ~ -onv o~-uer . 60-lnr so-oaa so-unr CD LO C\J 0 (1J6W) en c 0 :;; ca .... -c Cl) (J c 0 0 Cl) "C 'i: 0 .c 0 ,... .... Cl) -Cl) E 0 N .!!! Q. 0 0> 0 CXl < ~ ~ ··~ ~ 1 ~ ~ ~ ~ 0 ~ .l v .......4 ~~ 0 co 0 0 L{) "'" (1J6W) 0 C\J 0 ,- - - - 0 v~-unr 8 ~-/\ON 8 ~ -ABV\1 ~~-des o ~-Bnv o~-uer so-oaa fl) c 0 ; Jo.. -c Cl) (.) c 0 0 Cl) -ca Jo.. ~ z N Jo.. Cl) a; E 0 N Cl) c.. ~ ------ ~ ...._ ~~ <0 0 ~ I!) 0 ..... ------ (1J6w) ....... \ ~ ~ ~. H ~ ~~ ~~ (\J 0 ,..... 0 17~-unr " £~-AON £ ~-ABII'J ~ ~-das o~-6nv o~-uer 6o-1nr -so-oaa so-unr 0 0 c 0 ~ -c Cl) (.) c 0 0 Cl) "'C 'i: _g .c 0 N """ Cl) G) E 0 N Cl) 0: co C\J T"" T"" v ~ ~ \. <. ~ ~ v· ~ \ '"' ... 0 (!) (1/6W) v~-unr 8 ~-AON ~~-des o ~ -onv o~-uer - ao-oaa 0 Ill s:::: 0 ·.;:: ca .... ... s:::: Cl) u s:::: 0 0 Cl) ... ca .... .1:::: z (W) .... Cl) ... Cl) E 0 N Cl) ii: ~-------r--------.-------~--------.-------~---------.v~-unr -8 ~-AON -c:a-Jd'v' ~ ~-das ~ ~-qa.:l o ~ -onv o~-uer eo-oaa ~-------r--------+--------+--------+-------~--------~Bo-unr (\J (1/6W) l[) 0 0 tn s:::: 0 '+=i cu ... -s:::: Cl) c.> s:::: 0 (.) Cl) "C 'i: 0 .s:::: (.) CW) ... Cl) -Cl) E 0 N .! ll. ~------~----~------~------~------~------~------~v~-unr 8 ~-/\ON 8 ~-ABV\1 · c~-PO G ~ -Jd'v' ~ ~-das ~ ~-qa.:J o ~ -onv -0~-uer 6o-1nr t.-------l~-----l-------+--------l--------4--------+--------+. ao-~aa 0 ""' ,..- 0 C\1 0 0 ,..- 0 00 (1J6W) 0 <0 0 ""' 0 C\1 0 tn c 0 ·~ 1: C1) u c 0 0 ~ :t::: z ,.... I z ~ 4~ ~ "' ~ " ~ (X) 0 (1/6W) ~ ~ • ~ ~ ~~ / v~ co 0 C\J 0 0 17~-unr 8~-AON 8 ~-ABV\1 ~ ~-das ~ ~-qa.:J o~-Bnv o~-uer eo-1nr so-oaa so-unr tn 1: 0 ·:::; m llo. -1: Cl) u 1: 0 0 Cl) "tJ 'i: .2 J: 0 ,.. I z 3: 1- ~------~--------~------~----------------~---------r v~-unr 8 ~-AON 8 ~ -fiBV\1 6 ~ -JdV ~ ~-das ~ ~-qa::i o ~ -Bnv o~-uer ~-------+--------+--------4--------4--------4---------+so-unr 0 ('I) Li) C\J 0 C\J 0 (1/6W) rn s::::: 0 ; ca ... -s::::: Q) u s::::: 0 (.) Q) -ca ... :t::: z ~ z 3: 1- ~-------.---------r--------.---------.--------.---------.v~-unr 8 ~-AON G ~ -Jd'v' ~ ~-das ~ ~ -qa:J . o~-onv o~-uer -6o-1nr so-oaa ~-------+--------+-------~--------4-------~---------+Bo-unr 0 (\j 0 0 ...- 0 a:> 0 <0 (1J6W) 0 (\j 0 1/) t: 0 ... ca ... -t: C1) u t: 0 0 C1) "C "i: 0 .c 0 N I z ~ r-------~---------.--------.---------r-------~---------r v~-unr 8~-AON c ~ -JdV ~ ~-das -~ ~-qa.:J o ~ -5nv o~-uer 5o-1nr so-oaa ~-------+--------+--------+--------~------~--------4 80-unr 0 N T""" 0 0 0 co 0 CD (1J6W) 0 N 0 "' t: 0 :;:; ca .... -t: C1) u t: 0 0 C1) -ca .... :!::::: z C") I z 3: 1- ~------r-------~------.-------,-------~-------r-------r v~-unr 8 ~-/\ON c ~ -Jdy -~ ~-das -~ ~-qa~ o ~-5ny o ~-uer so-::>ao ~----~~----~------~-------+-------r------~-------+80-unr U') ('I) U') C\J 0 C\J U') 0 (1f6W) VI s::: 0 ·.;::o cu I.. -s::: Cl) C.> s::: 0 0 Cl) 'C 'i: 0 .s::. 0 ('I) I z == 1- ~----~----~----~----~----~------r-----~----~-----r v~-unr -8~-AON c ~ -Jd'Q' .. ~~-des • ~ ~-qa.:J N-5ny o ~-uer · 60·1nr ~----~----+-----+-----+-----~----~----~----~-----+90-unr 0 co T"" 0 CD 0 C\J 0 0 T"" 0 co (1J6W) 0 CD 0 '<:1" 0 C\1 0 tn c 0 +:0 cu "--c Cl) (,) c 0 (.) Cl) -cu "-.'!:::: z -.:t I z 3: t- ~----~----~-----r----~----~~----~----~----~-----r v~-unr 8 ~-AON <:: ~ -JdV -~~-des ~ ~-qa.:J o ~ -5nv o ~-uer 6o-1nr so-oaa ~----+-----+-----+-----4-----4-----4-----4-----4------+so-unr .,..... <Xl 0 (1t6w) (!) 0 "! 0 0 en c 0 '+=i ctl ... .... c Cl) (,) c 0 (.) Cl) "C 'i: 0 .c (.) "':t I z ~ 1- ~-----.------~----~------~-----,------~----~r------r v~-unr 8~·AON • G ~ -Jd'v' ~ ~-das ~ ~ -qa.:J o ~ -onv o~·uBr -60·1nr so-oaa ~----~-----4------+------+------+-----~----~~----+so-unr 0 (t) LO C\1 0 C\1 {1t6w) LO 0 LO 0 ,..... ,..... ~---------r----------.----------.----------r----------r v~-unr £~-/\ON £ ~-AeV\1 c~-PO en c 0 '.j:i G ~-Jd'v' ctl ""' ... c Cl) (,) c 0 0 Cl) ~ ~-das ... ctl ""' .'!:::: z r-.. I z ~ 1-~ ~-qa.:J -oH>nv o ~-u-er 1------4-------4------+------+------t-5o-1nr It) 0 c:i r--------T--------~-------.--------,--------,--------~v~-unr £~-AON -£ ~-keV\1 tn r::::: G ~ -Jd'v' 0 +:0 m 1.. -r::::: Cl) (,) r::::: ~ ~-das 0 0 Cl) "'C 'i: 0 J: 0 -~ ~-qa.::l ....... I z 3: 1- -o ~ -Bnv . 0~-u-er 6o-1nr ~------~--------+--------+--------+--------4--------+so-oaa (\J 0 (\J 0 ,..- (1f6W) U) s:::: 0 '+" cu :r.. -s:::: Cl) () s:::: 0 0 Cl) -cu :r.. :!::::: z co ,.... I z s: 1- r---------~----------r---------~----------r---------~v~-unr -8~-AON 8 ~-ABV\1 c~-PO c ~ -Jd'v' . ~ ~-das ~ ~ -qa.:J o ~ -Bnv -okuer 1----------r------+--------if--------+------1-eo-1nr C\1 (1J6W) l.() ci 0 In c: 0 ·.; m to.. -c: C1) 0 c: 0 0 C1) "0 ·.:::: ..2 .c: 0 co ,.... I z ~ r------r-----,.-----.-----~------.-----~------~-----r v~-unr 8~-AON 8 ~-ABII'J c~-PO • G ~ -Jd'v' -~ ~-das ~ ~-qa.::l o ~ -Bnv o ~-uer 1-----+-----+------l------+-----l-------4----l----+ 5o-1nr 0 ro 0 CD 0 It) 0 """ (1/6W) 0 C\J 0 0 0 0 0 7/1/2002 11/1/2002 3/1/2003 7/1/2003 11/1/2003 3/1/2004 7/1/2004 11/1/2004 3/1/2005 7/1/2005 11/1/2005 3/1/2006 7/1/2006 11/1/2006 3/1/2007 7/1/2007 - 11/1/2007 3/1/2008 7/1/2008 11/1/2008 3/1/2009 7/1/2009 - 11/1/2009 3/1/2010 7/1/2010 11/1/2010 3/1/2011 7/1/2011 11/1/2011 3/1/2012 7/1/2012 11/1/2012 3/1/2013 7/1/2013 ~ 0 8 N 0 0 0 w 0 0 0 ,f::o. 0 0 0 VI 0 0 0 0"1 0 0 0 -..J 0 0 0 -1 ~ ~ I ~ \D z -· ,.. ~ QJ ,.. tD n 0 ::::s n tD ::::s ,.. ~ QJ ,.. -· 0 ::::s (I) 0 12/1/2005 3/1/2006 6/1/2006 9/1/2006 12/1/2006 3/1/2007 6/1/2007 9/1/2007 12/1/2007 3/1/2008 6/1/2008 9/1/2008 12/1/2008 3/1/2009 6/1/2009 9/1/2009 12/1/2009 - 3/1/2010 6/1/2010 9/1/2010 - 12/1/2010 3/1/2011 6/1/2011 9/1/2011 12/1/2011 3/1/2012 6/1/2012 9/1/2012 12/1/2012 3/1/2013 6/1/2013 9/1/2013 ...... lJ1 0 0 0 ...... lJ1 0 I'.J 0 0 I'.J lJ1 0 -4 ~ ~ I ~ \D n :::r -0 .., -· a. tD n 0 :::s n tD :::s .... Ql .... -· 0 :::s "' 0 N -!:> CTl 0 0 0 0 5/1/2005 8/1/2005 11/1/2005 2/1/2006 5/1/2006 8/1/2006 11/1/2006 2/1/2007 5/1/2007 8/1/2007 11/1/2007 - 2/1/2008 5/1/2008 8/1/2008 11/1/2008 2/1/2009 - 5/1/2009 8/1/2009 11/1/2009 2/1/2010 5/1/2010 8/1/2010 11/1/2010 2/1/2011 . 5/1/2011 8/1/2011 11/1/2011 2/1/2012 5/1/2012 8/1/2012 11/1/2012 2/1/2013 5/1/2013 8/1/2013 11/1/2013 00 0 ...... 0 0 ...... N 0 ...... -!:> 0 ...... CTl 0 ~ ~ I N ..... z -· r+ ... OJ r+ tD n 0 ::::s n tD ::::s r+ ... OJ r+ -· 0 ::::s U\ 0 12/1/2005 - 3/1/2006 6/1/2006 9/1/2006 12/1/2006 3/1/2007 - 6/1/2007 . 9/1/2007 12/1/2007 3/1/2008 . 6/1/2008 9/1/2008 12/1/2008 3/1/2009 6/1/2009 9/1/2009 12/1/2009 3/1/2010 6/1/2010 9/1/2010 12/1/2010 3/1/2011 6/1/2011 9/1/2011 12/1/2011 3/1/2012 6/1/2012 9/1/2012 12/1/2012 3/1/2013 6/1/2013 9/1/2013 l.n 0 ....... 0 0 ....... l.n 0 N 0 0 N l.n 0 w 0 0 w l.n 0 ~ 0 0 -1 ~ ~ I N ..... n ::r -0 .., -· a. tD n 0 :::J n tD :::J ,.... Ql ,.... -· 0 :::J "' ..... lia E TW4-22 Nitrate Concentrations 70 60 so 40 30 20 t"--• • d I • v \.:: . • I 10 0 2/28/2007 2/29/2008 2/28/2009 2/28/2010 2/28/2011 2/29/2012 2/28/2013 "' c 0 ·-...., rtJ .... ...., c cu u c 0 u cu "'C ·-.... 0 ..c u N N I lll::t s .... 0 0 I'- 0 0 1.0 0 0 Ll'l 0 0 o::t 1/SW 0 0 ("(') 0 0 N 0 0 .-I ("(') .-I 0 N ~ N -N N .-I 0 N -(J) N -N .-I .-I 0 N -00 N -N 0 .-I 0 N -00 N -N (J) 0 0 N -00 N -N 00 0 0 N -(J) N -N so 45 40 35 30 ..... liD 25 E 20 15 10 5 0 6/27/2007 TW4-24 Nitrate Concentrations 6/27/2008 6/27/2009 6/27/2010 6/27/2011 6/27/2012 6/27/2013 ..... bo E 1400 1200 1000 800 600 400 200 0 6/27/2007 TW4-24 Chloride Concentrations 6/27/2008 6/27/2009 6/27/2010 6/27/2011 6/27/2012 6/27/2013 U') c 0 ·-...., "' '-...., c cu u c 0 u cu ...., "' '-...., ·-z Ln N I q-s .... Ll') N 0 N Ll') .-f 1/SW 0 .-f .-f .-f 0 N -I' N -1.0 0 .-f 0 N -I' N -1.0 0'1 0 0 N -I' N -1.0 00 0 0 N -I' N U5" I' 0 0 N -I' oN U5" "' c 0 ·-+"' nJ .... +"' c cv u c 0 u cv "'C ·-.... 0 ..c: u Ln N I q-s 1- 0 0 0 0 Lfl 0 Lfl 0 <:t <:t !"(') !"(') 0 0 0 0 Lfl 0 Lfl 0 N N .-i .-i 1/~W 0 0 Lfl N .-i 0 N -r-. N ~ .-i .-i 0 N -r-. N -1.0 0 .-i 0 N -r-. N -1.0 O'l 0 0 N -r-. N -1.0 00 0 0 N r:::- N ~ r-. 0 0 N -r-. N -1.0 0 0 6/1/2005 9/1/2005 12/1/2005 3/1/2006 6/1/2006 9/1/2006 12/1/2006 3/1/2007 6/1/2007 9/1/2007 12/1/2007 3/1/2008 6/1/2008 - 9/1/2008 12/1/2008 .. 3/1/2009 .. 6/1/2009 9/1/2009 12/1/2009 3/1/2010 6/1/2010 9/1/2010 12/1/2010 3/1/2011 - 6/1/2011 ~ 9/1/2011 12/1/2011 3/1/2012 6/1/2012 •. 9/1/2012 12/1/2012 3/1/2013 6/1/2013 9/1/2013 12/1/2013 V1 0 ...... 0 0 ...... V1 0 "-1 0 0 "-1 V1 0 ~ :E I w 0 z -· r+ Ql r+ tt) n 0 :::::s n tt) :::::s r+ ""' DJ r+ -· 0 :::::s "' 0 6/1/2005 9/1/2005 12/1/2005 3/1/2006 . 6/1/2006 9/1/2006 12/1/2006 . 3/1/2007 6/1/2007 9/1/2007 12/1/2007 3/1/2008 6/1/2008 9/1/2008 12/1/2008 3/1/2009 6/1/2009 9/1/2009 12/1/2009 3/1/2010 - 6/1/2010 9/1/2010 12/1/2010 . 3/1/2011 6/1/2011 ~ 9/1/2011 12/1/2011 l 3/1/2012 _, 6/1/2012 9/1/2012 12/1/2012 3/1/2013 6/1/2013 9/1/2013 12/1/2013 N 0 -1>-0 en 0 00 0 ...... 0 0 ...... N 0 ...... -1>-0 ...... en 0 ...... 00 0 s: ~ I w 0 n :::r -0 ., -· c. t'D n 0 ::::s n t'D ::::s ..... Dl ..... -· 0 ::::s "' 0 0 . 6/1/2005 9/1/2005 12/1/2005 3/1/2006 6/1/2006 9/1/2006 12/1/2006 3/1/2007 •. 6/1/2007 9/1/2007 12/1/2007 3/1/2008 6/1/2008 . 9/1/2008 •. 12/1/2008 3/1/2009 6/1/2009 9/1/2009 12/1/2009 3/1/2010 6/1/2010 9/1/2010 12/1/2010 3/1/2011 . 6/1/2011 9/1/2011 12/1/2011 3/1/2012 6/1/2012 9/1/2012 12/1/2012 3/1/2013 6/1/2013 9/1/2013 12/1/2013 \.n 0 ..... 0 0 ..... \.n 0 N 0 0 N \.n 0 w 0 0 w \.n 0 s: :e I w t--ao z -· r-1" OJ r-1" tD n 0 :::s n tD :::s r-1" OJ r-1" -· 0 :::s "' 0 6/1/2005 9/1/2005 12/1/2005 3/1/2006 6/1/2006 - 9/1/2006 12/1/2006 3/1/2007 6/1/2007 9/1/2007 12/1/2007 3/1/2008 6/1/2008 9/1/2008 - 12/1/2008 3/1/2009 6/1/2009 9/1/2009 12/1/2009 3/1/2010 6/1/2010 9/1/2010 12/1/2010 3/1/2011 6/1/2011 9/1/2011 12/1/2011 3/1/2012 6/1/2012 - 9/1/2012 12/1/2012 - 3/1/2013 6/1/2013 9/1/2013 12/1/2013 V'l 0 1-' 0 0 1-' V'l 0 "-> 0 0 "-> V'l 0 s ~ I w t-a n ::r -0 ""'' -· c. tD n 0 ::J n tD ::J ,.... Ql ,.... -· 0 ::J "' TabL CSV Transmittal Letter Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Lundberg, Kathy Weinel Friday, February 21, 2014 9:08AM 'Rusty Lundberg' 'Phillip Goble'; 'Dean Henderson'; Harold Roberts; Frank Filas, P.E; David Frydenlund; Dan Hillsten; David Turk; Jaime Massey Transmittal of CSV Files White Mesa Mill 2013 04 Nitrate Monitoring 131 0396-EDD-rev1.csv Attached to this e-mail is an electronic copy of laboratory results for nitrate monitoring conducted at the White Mesa Mill during the fourth quarter of 2013, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel 1