DRC-2013-003059 - 0901a068803b3693

ENERGYFUELS "DRC-2013-003059"
Energy Fuels Resources (USA) Inc.
225 Union Blvd. Suite 600
Lakewood, CO, US, 80228
303 974 2140
www energytuels com
August 29, 2013
VIA OVERNIGHT DELIVERY
Mr. Rusty Lundberg
Director of the Utah Division of Radiation Control
State of Utah Department of Environmental Quality
195 North 1950 West
P.O. Box 144850
Salt Lake City, UT 84116-4850
CP
•o -
V-
Dear Mr. Lundberg:
Re: State of Utah Radioactive Material License No. UT1900479
White Mesa Mill, Blanding, Utah
Semi-Annual Effluent Monitoring Report for Period
January 1,2013 through June 30,2013
As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65
(subpartl)), and License Condition 11.3A of State of Utah Radioactive Materials License No.
UT 1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill
for the period January 1, 2013 through June 30, 2013.
If you have any questions regarding this report, please contact the undersigned at (303) 389-
4132.
Yours very truly,
ENERGY FUELS RESOURCES (USA) INC.
Jo Ann Tischler
Manager, Compliance and Licensing
cc: David C. Frydenlund
Harold R. Roberts
David E. Turk
Katherine A. Weinel
Central Files
August 29, 2013
VIA OVERNIGHT DELIVERY
Mr. Rusty Lundberg
Director of the Utah Division of Radiation Control
State of Utah Department of Environmental Quality
195 North 1950 West
P.O. Box 144850
Salt Lake City, UT 84116-4850
Dear Mr. Lundberg:
Energy Fuels Resources (USA) Inc.
225 Union Blvd. Suite 600
Lakewood, CO, US, 80228
303 974 2140
www .energyfuels.com
Re: State of Utah Radioactive Material License No. UT1900479
White Mesa Mill, Blanding, Utah
Semi-Annual Effluent Monitoring Report for Period
January 1, 2013 through June 30,2013
As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65
(subpart1)), and License Condition 11.3A of State of Utah Radioactive Materials License No.
UT1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill
for the period January 1, 2013 through June 30, 2013.
If you have any questions regarding this report, please contact the undersigned at (303) 389-
4132.
Yours very truly, r<-1/-~-~&A-
ENERGY FUELS RESOURCES (USA) INC.
J o Ann Tischler
Manager, Compliance and Licensing
cc: David C. Frydenlund
Harold R. Roberts
David E. Turk
Katherine A. Weinel
Central Files
White Mesa Uranium Mill
Radioactive Materials License UT900479
Semi-Annual Effluent Monitoring Report
(January through June 2013)
Prepared For:
Utah Department of Environmental Quality
Division of Radiation Control
Prepared by:
Energy Fuels Resources (USA) Inc.
225 Union Boulevard, Suite 600
Lakewood, CO 80228
August 29, 2013
Table of Contents
1.0 IN"TRODUCTION .................................................................................................. 1
2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLIN"G ...................................... 2
2.1 Program Overview ...................................................................................... , ........ 2
2.2 Sampling Protocol and Analytical Results ........................................................... 2
2.3 General Observations .................................................................... , ...................... 3
2.4 Site Specific Sampling Data ................................................................................. 4
2.5 Radon-222 ............................................................................................................ 6
3.0 EXTERNAL RADIATION (DIRECT GAMMA) .................................................. 7
4.0 VEGETATION SAMPLES ..................................................................................... 8
5.0 STACK SAMPLIN"G ............................................................................................... 9
6.0 SURFACE WATER MONITORIN"G .................................................................... 12
7.0 SOIL SAMPLIN"G ................................................................................................. 12
8.0 METEOROLOGICAL MONITORIN"G .............. , ................................................. 12
9.0 SIGNATURE .......................................................................................................... 13
LIST OF TABLES
Table 1 NCRP Report 94-Global Pb-210 Concentration Example
Table 2 Air Monitoring Station Results U-Nat (Comparison to Limits)
Table 3 Air Monitoring Station Results Th-230 (Comparison to Limits)
Table 4 Air Monitoring Station Results Ra-226 (Comparison to Limits)
Table 5 Air Monitoring Station Results Pb-210 (Comparison to Limits)
Table 6 Environmental OSL Dosimeter Measurements (Gamma)
Table 7 Stack Sampling Requirements
Table 8 Stack Effluent Concentrations and Release Rates
1
INDEX OF TABS
A High Volume Air Monitoring Stations
B BHV Air Sampling Graphs and Data Tables
Tab 1 BHV -1 Air Sampling Graphs and Data Table
Tab 2 BHV -2 Air Sampling Graphs and Data Table
Tab 3 BHV -3 Air Sampling Graphs and Data Table
Tab 4 BHV-4 Air Sampling Graphs and Data Table
Tab 5 BHV -5 Air Sampling Graphs and Data Table
Tab 6 BHV -6 Air Sampling Graphs and Data Table
C BHV Air Sampling Laboratory Results and QNQC
D Air Particulate Loading Graphs and Supporting Data
E Environmental Gamma (OSL) Dosimeter Graphs and Supporting Data
F Vegetation Graphs, Data Table, Laboratory Results and QNQC
G Stack Sample Laboratory Results
H Surface Water Graphs and Field Data Sheets
I Soil Sample Graphs, Data Table, Laboratory Results and QNQC
ii
WHITE MESA URANIUM MILL
SEMI-ANNUAL EFFLUENT REPORT, JANUARY THROUGH JUNE 2013
1.0 INTRODUCTION
The White Mesa Mill (the "Mill") has established monitoring programs to evaluate
compliance with effluent limitations and to assess the potential for release of radioactive
material into the local environment. These monitoring programs were developed and
implemented at the time of Mill construction, operated with appropriate adaptation over
time, and are consistent with the Mill's State of Utah Radioactive Materials License No.
UT1900479 (the "License") and guidelines developed by the United States Nuclear
Regulatory Commission ("NRC") (NRC Regulatory Guide 4.14, Radiological Effluent
and Environmental Monitoring at Uranium Mills-Rev. 1, ML003739941), 1980).
Under these programs, the Mill monitors the following environmental media and
conditions:
a) Airborne patticulate radionuclide concentrations obtained from the following
sampling stations:
• North, east and south of the Mill Site: BHV-1 and BHV-2 (north), BHV-5
(east), and BHV -4 (south). BHV -1 serves as a surrogate for the nearest
resident (BHV -1 is approximately 1.2 miles north of the Mill, but
approximately 0.4 miles closer to the Mill than the nearest resident);
• A background location distant to and west of the Mill (BHV-3), which
was monitored for airborne particulate up until November, 1995, at which
time background was established, but is no longer monitored for air
particulate; and
• A station specifically requested by the White Mesa Ute Community south
of the Mill Site (BVH-6);
b) External (direct) gamma radiation measured at air monitoring stations BHV -1,
BHV-2, BHV-3, BHV-4, BHV-5 and BHV-6;
c) Vegetation at three site periphery locations, for uptake of radiation;
d) Stack release rates from the Mill's air emissions sources;
e) Surface water at Cottonwood Creek and, when flowing, Westwater Creek, both
located west of the Mill;
f) Soil radionuclide activity obtained near the air particulate monitoring stations,
during the third quarter of each year;
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g) Groundwater (up and down gradient) of the Mill facility; and1
h) Seeps and springs in the vicinity of the Mill.1
This semi-annual effluent report provides the results of the specific monitoring and
sampling activities that were undertaken during the subject reporting period.
2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING
2.1 Program Overview
The environmental airborne particulate monitoring program at the Mill utilizes four air
sampling stations. Four high-volume continuous air sampling stations (BHV-1, BHV-2,
BHV-4, and BHV-5) are required by the License. These sampling stations serve as
sentinels for airborne particulate which could potentially emanate from the Mill site. In
addition to its general site monitoring function, BHV -1 also serves as a conservative
surrogate for concentrations at the nearest resident, because it is located approximately
1.2 miles north of the Mill just south of the nearest resident but between the Mill and that
resident.
With regard to background monitoring, the Mill previously operated a continuous high-
volume air sampling station (BHV-3) which was located approximately 3.5 miles west of
the Mill site. With the approval of NRC, this station (BHV-3) was removed from the
active air monitoring program in November 1995. At that time, NRC determined that a
sufficient air monitoring data base had been compiled at BHV-3 to establish a
representative airborne radionuclide background for the Mill. It should be noted,
however, that while air sampling was discontinued at this location, gamma measurements
and soil sampling continue at BHV-3.
In addition to the environmental air sampling locations described above, an additional
station (BHV -6) was installed at the request of the White Mesa Ute Community. This
station began operation in July of 1999 and provides airborne particulate information in
the southerly direction between the Mill and the White Mesa Ute Community.
2.2 Sampling Protocol and Analytical Results
Airborne particulate monitors are operated continuously at each of the high-volume air
sampling stations referenced above except BHV -3, as noted above. Particulate sample
collection filters are gathered by site technicians weekly in accordance with the Mill's
environmental air sampling procedures and are composited on a quarterly basis for
laboratory analyses. The collected filters are analyzed for Unat activity, Th-230 activity,
Ra-226 activity, and Pb-210 activity. Fugitive dust standards for the facility are limited
by the Mill's State of Utah Air Approval Order, which sets a 20% visual opacity
1 Groundwater sampling and seeps and springs sampling are reported separately pursuant to the Mill's State
of Utah Ground Water Discharge Permit No. UGW370004, and are not included with this report.
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standard. The specific locations of the Mill's airborne particulate monitoring stations are
depicted on the figure entitled High Volume Air Monitoring Stations included as
Attachment A. Station BHV -3, which is no longer sampled for air particulate, is located
approximately 3.5 miles west of the Mill facility and is not indicated on that Figure.
The analytical results of radionuclide particulate sampling for each monitoring station
operated during this reporting period are provided in Attachment B under separate
sampling station attachment tabs (Tabs 1-6). Each Tab contains graphical illustrations of
the radionuclide concentrations in log-scale presentation format. The graphs display
reported data over time since the 1981 inception of the Mill's environmental air
particulate monitoring program. The actual analytical results (and associated QA/QC
information) reported by the laboratory for the reporting period are provided under
Attachment C. In addition to the analyses for radionuclides, particulate loading is
determined for each filter and composited as a quarterly mass-loading estimate for review
purposes only. Graphs showing particulate loading at each station and the underlying data
are included as Attachment D.
It should be noted that for BHV-6 the first 2 sampling periods of 2012 have been omitted
from particulate loading on the graph in Attachment D. The timer on the airborne
particulate monitoring station at BHV -6 malfunctioned, and the data are considered
invalid due to the inability to measure the time sampled. The timer was replaced prior to
the third sampling period in 2012 and all other measurements are valid.
It should be noted that for graphical illustration purposes, values reported at zero, values
reported at less than the prescribed detection limit ( < 1 X 10-16 uCi/ml), and missing
values were plotted as 1 x 10-16 uCi/ml concentrations. Where other "less than" values
were indicated (i.e., where detection limits for the data varied from 1 x 10-16 uCilml), the
detection limit concentration was utilized for plotting the data point. This graphing
convention is not utilized to formulate station average information, nor is it intended as a
precedent for data treatment. Rather, the intent is to provide a conservative viewable
depiction of site airborne radionuclide information. This is considered to be a
conservative approach, because the actual concentration below the detection limit cannot
be determined and, as a result, the plotted point will be at the same or a higher
concentration than the actual activity concentration of the collected sample.
2.3 General Observations
The results of environmental air monitoring for this semi-annual period indicate that for
all radionuclides at all monitoring stations airborne radionuclide particulate activity
concentrations were well below regulatory Effluent Concentration Limits ("ECL's") and
the Mill's ALARA goals, which are set at 25% of the ECLs.
It is noteworthy and expected that Pb-210 concentrations are elevated when compared to
the other parent radionuclide concentrations (i.e. U-nat, Th-230 and Ra-226). This
phenomenon is due to the well-established controlling effect experienced worldwide as a
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result of the ubiquitous presence of radon in the earth's atmosphere. Accordingly,
elevated Pb-210 presence in disequilibrium with parent radionuclides measured here is
not associated with uranium milling operations. Rn-222 emanates as a decay-chain
progeny of the Ra-226 contained in the soil of the earth's crust and is dispersed generally
throughout the earth's atmosphere. The electrically charged short and long-lived decay
products of Rn-222 attach to ambient dust particles found naturally in the atmosphere and
are carried with the air. Pb-210 is the longest lived of these decay products and is the
decay product of the shorter-lived radon progeny. As such, it accumulates as an electrical
attachment on the natural ambient dust in the atmosphere and is generally measured at
elevated activity when compared to local decay-chain parent radionuclide activity,
regardless of uranium milling activity. At the Mill's BHV air monitoring stations, all
dust (ambient natural and mill derived) is collected by the sample filter. Because of the
natural elevation of Pb-210 accumulated as an attachment to the naturally occurring
ambient dust particles collected by the air sampling equipment, Pb-210 is commonly
elevated and in disequilibrium when compared to parent radionuclide activity, regardless
of the Mill's presence. By way of illustration, average ground-level concentrations have
been reported for selected States (NCRP Report 94, 1992) and are summarized in Table 1
below, demonstrating elevated Pb-210 activity where no uranium milling operations are
located nearby. In April 1977, prior to Mill construction and Mill operations, air
particulate Pb-210 was measured at the Mill site to be 1.3E-14 uCi/ml (13.0E-3 pCi/m3i.
Table 1-NCRP Report 94-Global Pb-210 Concentration Example
State Pb-210 Concentration
uBq/Mj uCi/ml
California 600 1.6E-14
Illinois 1500 4.1E-14
Ohio 300 S.lE-15
Massachusetts 700 1.9E-14
2.4 Site Specific Sampling Data
The results of airborne particulate monitoring for the period (without background
subtraction) are provided by sampling station and radionuclide in Tables 2 through 5
below. Along with these data, the tables present comparative ECL's and the ECL
percentage measured at each of the monitoring stations sampled during the period. A
review of these data supports the conclusion that airborne particulate is well controlled at
the Mill. In all cases, the measured activity concentrations were well within the ECL, as
well as the Mill's ALARA goal (i.e. 25% of the ECL). Lower Limits of Detection
consistent with NRC Regulatory Guide 4.14 were maintained by the Mill's contract
analytical laboratory for this reporting period.
2 See the Environmental Report, White Mesa Uranium Project, San Juan County, Utah for Energy Fuels
Nuclear, Inc. prepared by Dames & Moore, January 30, 1978, Section 2.9.1.1
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In fact, the data obtained since program inception in 1981 indicates that only one
individual quarterly measurement (Th-230 at BHV-5 for the 2nd Quarter of 1996) has
ever exceeded the ECL at the Mill. With regard to that particular single measurement,
while it is important to consider and evaluate an individual measurement exceeding the
ECL, for public dose estimation purposes, it is the average annual concentration that is of
primary significance. In that instance, the average annual concentration of Th-230 for
BHV-5 in 1996 was well below the ECL. Data obtained since program inception in 1981
also indicate that, with very few exceptions, the gross (background inclusive)
measurements do not exceed the site's ALARA goal (i.e. only nine of the several
thousand total gross radionuclide determinations to date exceeded the Mill's self-imposed
25 % ALARA goal).
Table 2-Air Monitoring Station Results U-Nat (Comparison to Limits) 1st and 2nd
Quarters 2013
Monitoring 1st Qtr. 2nd Qtr. Effluent Average ~
Station Result Result Concentration Percent
(uCilml) (uCilml) Limit (ECL) ECL
(uCi/ml)
BHVl 9.91E-16 1.46E-15 9.00E-14 1.36E+00
BHV2 3.38E-16 4.06E-16 9.00E-14 4.13E-01
BHV4 3.04E-15 2.50E-15 9.00E-14 3.08E+00
BHV5 6.66E-15 7.35E-15 9.00E-14 7.78E+00
BHV6 4.52E-15 5.91E-15 9.00E-14 5.79E+00
Table 3-Air Monitoring Station Results Th-230 (Comparison to Limits) 1st and 2nd
Quarters 2013
Monitoring 1st Qtr. 2nd Qtr. Effluent Average
Station Result Result Concentration Percent
(uCilml) (uCilml) Limit (ECL) ECL
(uCi/ml)
BHVl 1.86E-16 3.34E-16 2.00E-14 1.30E+00
BHV2 3.94E-17 4.89E-17 2.00E-14 2.21E-Ol
BHV4 4.99E-16 3.62E-16 2.00E-14 2.15E+00
BHV5 1.48E-15 1.72E-15 2.00E-14 8.00E+00
BHV6 7.93E-16 6.74E-16 2.00E-14 3.67E+00
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Table 4-Air Monitoring Station Results Ra-226 (Comparison to Limits) 1st and 2nd
Quarters 2013
Monitoring 1st Qtr. 2nd Qtr. Effluent Average
Station Result Result Concentration Percent
(uCi/ml) (uCi/ml) Limit (ECL) ECL
(uCi/ml)
BHVl 2.04E-16 3.91E-16 9.00E-13 3.31E-02
BHV2 8.32E-17 8.06E-17 9.00E-13 9.10E-03
BHV4 2.79E-16 2.40E-16 9.00E-13 2.88E-02
BHV5 1.12E-15 2.02E-15 9.00E-13 1.74E-01
BHV6 4.91E-16 7.85E-16 9.00E-13 7.09E-02
Table 5-Air Monitoring Station Results Pb-210 (Comparison to Limits) 1st and 2nd
Quarters 2013
Monitoring lst Qtr. 2nd Qtr. Effluent Average
Station Result Result Concentration Percent
(uCi/ml) (uCi/ml) Limit (ECL) ECL
(uCi/ml)
BHVl 1.82E-14 5.78E-15 6.00E-13 2.00E+00
BHV2 1.42E-14 4.93E-15 6.00E-13 1.59E+00
BHV4 2.13E-14 4.93E-15 6.00E-13 2.19E+00
BHV5 1.80E-14 6.67E-15 6.00E-13 2.06E+00
BHV6 1.70E-14 5.18E-15 6.00E-13 1.85E+00
2.5 Radon-222
Due to the unavailability of monitoring equipment to detect the revised 10 CFR Part 20
standard, and with the approval of NRC, Radon 222 monitoring at BHV stations was
discontinued in 1995. Instead, compliance with these limits and the requirements of
R313-15-301 is demonstrated by a calculation, authorized by the NRC and as
contemplated by R313-15-302(2)(a). A copy of the Technical Evaluation Report
evidencing such approval was enclosed with correspondence to the Division of Radiation
Control ("DRC") on July 28, 2008.
This calculation is performed by use of the MILDOS code for estimating environmental
radiation doses for uranium recovery operations (Strenge and Bender 1981) and more
recently in 2003 by use of the updated MILDOS AREA code (Argonne 1998). The
analysis under both the MILDOS and MILDOS AREA codes assumes the Mill to be
processing high grade Arizona Strip ores at full capacity, and calculates the
concentrations of radioactive dust and radon at individual receptor locations around the
Mill.
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The MILDOS and MILDOS AREA codes calculate the combined Total Effective Dose
Equivalent ("TEDE") from all relevant pathways, including both air particulate and
radon, at a number of locations including the nearest residence (the individual likely to
receive the highest dose from the licensed operation), approximately 1.6 miles north of
the Mill. These calculations reveal projected doses to the individual likely to receive the
highest dose from the licensed operations to be well below the 100 mrem regulatory limit
in R313-15-301(1)(a) for all pathways, including air particulate and radon, and well
below the ALARA goal of 10 mrem/yr for air emissions excluding radon as set out in
R313-15-101(4). MILDOS AREA modeling was recently conducted in support of the
Mill's 2007 License Renewal Application, utilizing the MILDOS-AREA code (Version
2.20~), to estimate the dose commitments at various receptor locations for processing of
Colorado Plateau ore (0.25% U30 8 and 1.5% V20 5) and Arizona Strip ore (0.637%
U30 8). The process rate was assumed to be at full capacity of 730,000 tons per year (an
average of 2,000 tons per day) with an average uranium recovery yield of 94%. That
modeling showed a TEDE of 2 mrem per year at the nearest resident (3 mrem per year at
the nearest potential residence, being the location of BHV -1 at the northern property
boundary of the Mill site), which included the dose from all radionuclide sources,
including radon. The modeled dose from radon itself was therefore a fraction of TEDE
and well within the regulatory limits.
3.0 EXTERNAL RADIATION (DIRECT GAMMA)
Gamma exposure rate estimates were measured for the reporting period utilizing passive
integrating devices, optically stimulated luminescence dosimeters ("OSLs"). These
dosimeters were located at each of the Mill's high-volume air sampling stations (BHV -1,
BHV-2, BHV-4, BHV-5 and BHV-6) and at the designated background monitoring
station (BHV -3). Measurements obtained from location BHV -3 have been designated as
background due to BHV-3's remoteness from the Mill site (i.e. BHV-3 is located
approximately 3.5 miles west of the Mill site). The results of the environmental OSL
measurements and semi-annual cumulative above-background data are provided in Table
6 below. In addition, measurement data obtained at these locations are graphically
presented at Attachment E to this report.
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Table 6-Environmental Optically Stimulated Luminescence Dosimeter
~easurements((;amma)
Monitoring 1st Qtr 2nd Qtr 1st Qtr 2nd Qtr Cumulative
Station Result Result 1 Result Less Result Less 1 Semi-
(mrem) (mrem) Background Background Annual
(mrem) (mrem) Estimate*
(mrem)
BHV1 32.0 32.7 4.8 5.0 9.8
BHV2 27.8 28.9 0.6 1.2 1.8
BHV3 27.2 27.7 0.0 0.0 0.0
BHV4 27.5 30.8 0.3 3.1 3.4
BHV5 30.0 30.9 2.8 3.2 6.0
BHV6 25.7 58.0 -1.5 30.3 30.3
*Negative values treated as zero for cumulative dose
The results for this period indicate that above background measurements for stations
BHV-1, BHV-2, BHV-4, BHV-5 and BHV-6 are within regulatory limits. BHV-1 is at
the location of the nearest potential residence. The nearest actual residence is
approximately 0.4 miles north of BHV -1. The annual individual member of the public
limit is 100 rnrem/yr for combined internal and external exposure.
As shown in Table 6 above, the second quarter result from BHV-6 was above historic
values, and an investigation into the potential source was conducted. There was no site
activity, or change in activity, at the Mill during the second quarter that could cause this
type of result. EFRI believes this value is the result of a laboratory error, because it is
clearly anomalous relative to all historic data.
4.0 VE<;ETATION SA~PLES
Vegetation samples are collected at three locations around the Mill property. The
sampling locations are: 1) nmtheast, 2) northwest and 3) southwest of the Mill facility.
The NRC Regulatory Guide 4.14 requires that three samples be collected during the
grazing season, without specifying exact months or times during the season. During the
2013 grazing season, two sets of samples were collected on April 30, 2013 and June 20,
2013. A third set of samples is planned for the fall season. The data from the fall season
sampling will be included in the July through December 2013 Semi-Annual Effluent
Report ("SAER") which will be submitted to the DRC on March 1, 2014. Data from the
April and June sampling events are included in this report.
Graphical log-scale presentation of the vegetation sampling results, together with the
analytical results reported by the Mill's contract laboratory (including QA/QC
information) for this sampling period, are included at Attachment F of this report. The
2013 data results are within the variation of previous sampling episodes.
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5.0 STACKSAMPLING
Under Section 5.0 of Tab 1.4 of the Mill's Environmental Protection Manual, Revision:
EFR-3, 12112 (the "Environmental Protection Manual") gas stack samples are collected
at the Mill in accordance with the calendar year schedule shown below:
Table 7 -Stack Sampling Requirements
Frequency Feed Stack (Grizzly Stack for Packaging
Baghouse) Yellowcake Dryer (Yellowcake
Baghouse)
Quarterly None If operating, U-nat If operating, U-nat
Semi-annually If operating, U-nat, If operating, U -nat, If operating, U-nat,
Th-230 Th-230, Ra-226, Pb-Th-230, Ra-226,
210 Pb-210
The Mill did not operate during January 2013. The grizzly baghouse operated
periodically during February and March 2013. The south yellowcake dryer and
yellowcake packaging baghouse operated only intermittently during February and March
2013 due to multiple dryer equipment shutdowns. As a result of the repeated startups and
shutdowns, the dryers only achieved representative steady state conditions, suitable for
stack monitoring, for approximately the last week in March (March 25-31), as discussed
in detail below.
The south yellowcake dryer, yellowcake baghouse, and grizzly baghou c operated during
the 2nd quarter of 2013. The north yellowcake dryer has not been in operation jnce the
3rd quarter of 2012, and therefore, has not been sampled since it wa Ia t jn operation.
NRC Regulatory Guide 4.14 requires that stack sampling should be "isokinetic,
representative, and adequate for determination of release rates and concentrations of
uranium." Due to operational conditions at the Mill during the 1st quarter of 2013, EFRI
was unable to achieve the steady state required for representative stack sampling at the
yellowcake dryers and the yellowcake baghouse as required by NRC Regulatory Guide
4.14. EFRI field personnel originally scheduled the sampling event with the stack
sampling contract company, Technical Emissions Testing Company ("TETCO"), on
February 19-21, 2013. The yellowcake dryers were shut down due to equipment issues on
February 18, 2013 and did not become operational again until February 22, 2013.
TETCO was unable to conduct the scheduled stack sampling at that time, and
rescheduled with EFRI field personnel to conduct sampling on March 4, 2013.
When TETCO returned on March 4, 2013, they were unable to conduct sampling again,
because the yellowcake dyers had been shut down and required equipment maintenance.
The yellowcake dryers continued to have operational issues sporadically during March of
2013. EFRI field personnel contacted TETCO on March 25, 2013 in an attempt to
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schedule a sampling event during the 1st quarter of 2013; however, TETCO was not
available to return to the Mill during the last week of March. Operation during the first
quarter was so sporadic that, despite three attempts, it was not possible to have TETCO
on site for the few days that the dryers were operating at conditions suitable for testing.
Due to the operational conditions in the 1st quarter of 2013, the 2nd quarter samples were
taken very early in the quarter, which resulted in a miscommunication with the analytical
laboratory. The yellowcake packaging baghouse was analyzed for only U-nat, as is
required for the first quarterly sample, excluding the analyses for Th-230, Ra-226, and
Pb-210 as is routinely performed for the second quarter samples. EFRI's QA Manager
identified the issue, noted that the sample were still within the method specified holding
time, and requested the laboratory analyze the samples for all required analyses. As a
result, all required analyses for the second quarter samples have been completed.
However, the laboratory was unable to deliver the Th-230, Ra-226, and Pb-210 results for
the yellowcake packaging baghouse in time to be included in this report. The complete
analytical data and the 2nd quarter 2013 results for Table 8, below, will be provided in a
separate addendum to this report after EFRI receives TETCO's report and analytical data.
The available analytical results of stack sampling conducted for the 2nd quarter of 2013,
as well as for the 3rd and 4th quarters of 2012, are provided in Table 8 below, indicating
the uCi/cc concentration in the stack emissions and the stack's radionuclide release rate
(uCi/sec) for U-Nat, Th-230, Ra-226 and Pb-210 at each of the stacks sampled. The
partial analytical results received to date, reported by the laboratory for the 2n quarter of
2013 are provided in Attachment G to this report.
It is also important to note that stack effluent concentrations are not comparable to
environmental air sampling station ECL's for regulatory compliance purposes. The ECL
is a limit that applies to the receptor locations and is not applicable to effluents from mill
processes on the Mill site. These stack release data are more appropriately utilized for
dose modeling purposes, and dose modeling is not computed for semi-annual reporting
purposes.
10
N:\WMM\Required Reports\Semi Annual Effluent Reports\2013 Jan-Jun\Jan_June 2013_SAER_text.docx
Table 8-Stack Effluent Concentrations and Release Rates
U-Nat U-Nat. Th-230 Th-230 Ra-226 Ra-226 Pb-210
u/Ci/cc uCi/sec uCi/cc uCi/sec uCi/cc uCi/sec uCi/cc
3rd Qtr, 2012
North YC 8.46E-09 5.51E-03 Not Not Not Not Not
Dryer, Run 1 Required Required Required Required Required
North YC 6.56E-09 4.49E-03 Not Not Not Not Not
Dryer, Run 2 Required Required Required Required Required
,
Not Not Not Yellowcake 1.19E-09 1.71E-03 Not Not
Baghouse Required Required Required Required Required
4th Qtr, 2012*
South YC l.J2E-08 5.60E-03 1.54E-13 7.72E-08 1.37E-14 6.84E-09 3.25E-12 Dryer, Run 1
South YC 1.13E-08 6.75E-03 2.45E-12 1.47E-06 2.13E-14 1.28E-08 2.27E-12 Dryer, Run 2
Yellowcake 3.04E-09 3.32E-03 1.15E-11 1.25E-05 7.80E-14 8.50E-08 3.64E-13 Baghouse
Grizzly Not Not Not
Baghouse 2.38E-ll l.l3E-05 2.17E-13 1.04E-07 Required Required Required
1st Qtr, 2013*
South YC EFRI was unable to Not Not Not Not Not
Dryer, Run I sample in the 1st Required Required Required Required Required
South YC quarter of 2013 due to Not Not Not Not Not
Dryer, Run 2 operational conditions Required Required Required Required Required
at the Mill. See Section
Yellowcake 5.0 above for a more Not Not Not Not Not
Baghouse detailed explanation. Required Required Required Required Required
2nd Qtr, 2013* I
South YC
Dryer, Run 1 2.94E-09 2.61E-03 8.51E-14 7.55E-08 3.01E-18 2.67E-12 3.59E-13
South YC
Dryer, Run 2 2.86E-09 2.56E-03 8.75E-14 7.85E-08 1.54E-17 1.38E-11 3.95E-13
Yellowcake ** ** ** ** **
Baghouse 3.93E-08 6.29E-02
Grizzly Not Not Not
Baghouse 1.68E-ll 1.11E-05 1.80E-13 1.18E-07 Required Required Required
*The North Yellowcake Dryer was not in operation during the 4111 quarter of 2012, or the 1" and 2"d
quarters of 2013.
Pb-21 0
uCi/sec
Not
Required
Not
Required
Not
Required
1.63E-06
1.36E-06
3.97E-07
Not
Required
Not
Required
Not
Required
Not
Required
3.19E-07
3.54E-07
**
Not
Required
**Due to laboratory error, these data were not available prior to the due date for this SAER, September 1,
2013. EFRI will submit an addendum to this SAER as soon as these data are available.
11
N:\WMM\Required Reports\Semi Annual Effluent Reports\2013 Jan-JunVan_June 2013_SAER_text.docx
6.0 SURFACE WATER MONITORING
Under the License, Part 11.2 B surface water samples are required to be obtained
annually from Westwater Canyon and semi-annually from Cottonwood Creek. Sediment
samples from Westwater Canyon are taken in place of the Westwater Canyon surface
water sample where surface water is not available for sampling. Westwater Canyon
surface water was not sampled in the first or second quarter of 2013, because no water
was present during this reporting period. Attempts to collect a surface water sample from
Westwater Canyon will continue through the next reporting period. If no surface water is
available, a sediment sample will be collected as required.
The Mill's Environmental Protection Manual requires that samples from Cottonwood
Creek be analyzed for total dissolved solids ("TDS") and total suspended solids ("TSS")
quarterly, and the License, Part 11.2 B requires that samples from Cottonwood Creek be
analyzed for dissolved and suspended radionuclides including Gross Alpha, U-nat, Ra-
226, and Th-230 semi-annually. In accordance with these requirements, Cottonwood
Creek was sampled for TDS and TSS during the 1st quarter, and was sampled for TDS,
TSS, and all radionuclides during the 2"d quarter.
The field data sheets for the surface water sampling events, along with graphs showing
historic results are included as Attachment H. The results of this sampling indicate that
surface water results remain low and within the range of typical background.
7.0 SOIL SAMPLING
Under Tab 4.1 of the Mill's Environmental Protection Manual, surface soils are required
to be sampled at the Mill's air monitoring stations (BHV-1, BHV-2, BHV-3, BHV-4,
BHV -5 and BHV -6) once per year during August or as soon as possible thereafter, but no
later than September 30 of each year. In accordance with the Mill's Environmental
Protection Manual, surface soils will be collected during the third quarter of 2013 and
will be discussed in the July through December 2013 report.
8.0 METEOROLOGICAL MONITORING
As in prior reporting periods, an independent contractor has prepared the White Mesa
Mill Semi-annual Meteorological Monitoring Report for the period of January through
June 2013. This information is retained at the Mill site for agency review.
12
N:\WMM\Required Reports\Semi Annual Effluent Reports\2013 Jan-Jun\Jan_June 2013_SAER_text.docx
9.0 SIGNATURE
This report was prepared by Energy Fuels Resources (USA) Inc. on August 29, 2013.
Energy Fuels Resources (USA) Inc.
Harold R. Roberts
Executive Vice President and Chief Operating Officer
13
N:\WMM\Required Reports\Semi Annual Effluent Reports\2013 Jan-Jun\Jan_June 2013_SAER_text.docx
ATTACHMENT A
HIGH VOLUME AIR MONITORING STATIONS
W:\lJSti\UTJ\l-1\Mill~, Pfans\AI!d'lan 3.2 2..3-f Nr "" 1.6 2.3-1 31/1012011
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I --~ : I _, \ ) r.s:. I ~~ ' 0 \ \ <J\: I ..(... I _______ l ___ \ : BHV-41 BHV-6 .. t;;.( ,, J -"0 : l ( i 1 ------------r-----------------------------~~~~k:_\_ t ---------
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'~-1411r I #.a I '• ' ' ) ....... ~-·!....-I '"lt \_, • _, ._ I ... _ ~ -:. ''-'----""" ... _...,. ~ '\ ., .. : l ,.. ...., ....... \ I -~ ., .. ..., "" \ .. ( i l \ \ ----_J·;--·------,--:---------------------(-----.....
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1 ( :.,'~ ~
\
_ .. _ .. _
-'-------~ -"' iL-~--· --
Property Boundary
Reservation Boundary
Canyon Rim
0 Air Monitor
Stations
Project
REVISIONS
Date I Bv
11109 •
1113/11 BM
11Z1111 BM
312112 GM
r
I
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Energy Fuels Resoutces (USA) Inc.
WHITE MESA MILL
COUnty. SAN JUAN Slabl: UT
LC~C<~Uon;
High Volume Air Monitoring Stations
,
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-B. Munkhbaatar
ATTACHMENT B
BHV AIR SAMPLING GRAPHS AND DATA TABLES
TAB 1
BHV-1 AIR SAMPLING GRAPHS AND DATA TABLE
Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-1U Effluent Concentration Limit= 2E-14 uCi/ml BHV-lT Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = 6E-13 uCi/ml BHV-1PB
ALARAGoal = 2.25E-14 uCi/ml AlARA Goal= SE-13 uCi/ml AlARAGoal = 2.25E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml
Pre 1994 MPC Limit= SE-12 uCi/ml pre '1.994'1W'Cllm1t= SE-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml
Pre 1994 A LARA GOAL= 1.2SE-12 uCi/ml Pre 1994 A LARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL= 1E-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
9/28/1981 2.35E-15 S.OOE-12 1.25E-12 7,82E-16 8.00E-14 2.00E-14 1.06E-15 2.00E-12 S,OOE-13 2,57E-14 4.00E-12 1.00E-12
12/14/1981 1.56E-15 S.OOE-12 1.25E-12 1.49E-15 S.OOE-14 2.00E-14 1,93E-15 2.00E-12 S.OOE-13 2.64E-14 4.00E-12 l.OOE-12
3/29/1982 2.16E-15 ~.OOE-12 1.25E-12 2.93E-15 B.OOE-14 2.00E-14 1.16E-15 2.00E-12 5.00E-13 2.09E-14 4.00E-12 l.OOE-12 I
6/30/1982 4.69E-15 5.00E-12 1.25E-12 3.46E-15 S.OOE-14 2.00E-14 2.38E-15 2.00E-12 5.00E-13 2.14E-14 4.00E-12 1.00E-12 '
9/27/1982 4.45E-15 S.OOE-12 1.25E-12 3.29E-15 B.OOE-14 2.00E-14 3.23E-15 2,00E-12 5,00E-13 1,99E-14 4,00E-12 1.00E-12 I
1/3/1983 4.39E-15 S.OOE-12 1.25E-12 5.91E-16 8.00E-14 2,00E-14 9.14E-16 2.00E-12 5.00E-13 4.87E-14 4.00E-12 l.OOE-12
4/4]1983 7.51E-16 5.00E-12 1.25E-12 2.13E-16 8.00E-14 2.00E-14 3.20E-16 2.00E-12 S.OOE-13 1.88E-14 4.00E-12 l.OOE-12
6/30/1983 2.68E-16 S.OOE-12 1.25E-12 6.92E-16 8.00E-14 2.00E-14 7.92E-16 2.00E-12 5.00E-13 2.00E-14 4.00E-12 l.OOE-12
10/3/1983 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 O,OOE+OO 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
1/3/1984 2.87E-15 S.OOE-12 1.25E-12 1.14E-16 8.00E-14 2.00E-14 l.79E-16 2.00E-12 5.00E-13 1,06E-14 4.00E-12 1,00E-12
4/2/1984 1.59E-15 S.OOE-12 1.25E-12 3 40E-16 8.00E-14 2.00E-14 3.71E-16 2-00E-12 S.OOE-13 3.34E-14 4.00E-12 l.OOE-12
7/2/1984 3.10E-15 S.OOE-12 1.25E-12 1.00E-1S 8.00E-14 2.00E-14 2.09E-15 2.00E-12 S.OOE-13 1.88E-14 4.00E-12 l.OOE-12
10/1/1984 6.42E-16 5.00E-12 1.25E-12 1.39E-16 8.00E-14 2.00E-14 l.94E-16 2-00E-12 S.OOE-13 1.85E-14 4.00E-12 l.OOE-12
1/2/1985 5.06E-16 S.OOE-12 1.25E-12 4.56E-16 8.00E-14 2-00E-14 3.49E-16 2.00E-12 S.OOE-13 3.03E-14 4.00E-12 l.OOE-12
4/1/1985 O.OOE+OO S.OOE-12 1.25E·12 1.23E-15 8.00E-14 2-00E-14 4.88E-16 2.00E-12 S.OOE-13 8.06E-15 4.00E-12 l.OOE-12
7/1/1985 7.17E-16 S.OOE-12 1.2SE·12 8.00E-14 2.00E-14 1.05E-15 2.00E-12 S.OOE-13 2.15E-14 4.00E-12 l.OOE-12
9/30/1985 6.13E-16 5.00E-12 1.25E-12 1.18E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 S.OOE-13 3.64E-15 4.00E-12 l.OOE-12
1/2/1986 3.42E-15 5.00E-12 1.25E-12 4.74E-16 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E·12
4/1/1986 3.98E-15 S.OOE-12 1.25E·12 9.74E-16 8.00E-14 2.00E-14 l.SOE-15 2.00E-12 S.OOE-13 1.41E-14 4.00E-12 l.OOE-12
6/30/1986 S.51E-17 5.00E-12 1.2SE·12 3.52E-16 8.00E-14 2.00E-14 1.37E-15 2.00E-12 S.OOE-13 1.23E-14 4.00E-12 l.OOE-12
10/27/1986 1.99E-15 5,00E-12 1.25E-12 3.06E-16 8,00E-14 2.00E-14 1.25E-15 2.00E-12 S,OOE-13 108E-14 4,00E-12 l.OOE-12
12/15/1986 1.67E-15 5,00E-12 1.25E-12 1.16E-16 8.00E-14 2.00E-14 5.98E-16 .2.00E-12 5.00E-13 1.37E-14 4.00E-12 l.OOE-12
3/16/1987 2.33E-15 S,OOE-12 1.2SE·12 4.30E-16 B.OOE-14 l .OOE-14 1.92E-16 2.00E-12 S.OOE-13 5.59E-14 4.00E-12 l.OOE-12
5/11/1987 2.36E-15 5.00E-12 1.25E-12 7.69E-16 8.00E-14 l .OOE-14 8.76E-16 2.00E-12 5.00E-13 1.45E-14 4.00E-12 l.OOE-12
9/9/1987 2.27E-15 5.00E-12 1.25E·12 2.44E-15 B.OOE-14 2.00E-14 8.51E-16 2.00E-12 5.00E-13 3.14E-14 4.00E-12 l.OOE-12
11/2/1987 2.75E-15 S.OOE-12 1.2SE·12 2.46E-15 8.00E-14 2.00E-14 1.34E-15 2.00E-12 5.00E-13 2.79E-14 4.00E-12 l.OOE-12
2/16/1988 1.07E-15 S.OOE-12 1.25E-12 1.47E-16 8.00E-14 2.00E-14 4.44E-16 2.00E-12 S.OOE-13 4,01E-14 4.00E-12 1.00E-12
5}18/1988 1.98E-15 5.00E-12 1.25E·12 1.25E-15 8.00E-14 2.00E-14 6.40E-16 2.00E-12 S.OOE-13 1,07E-14 4.00E-12 l.OOE-12
8}15/1988 2.06E-15 5.00E-12 1.25E·12 3.41E·15 8.00E-14 .2.00E-14 5.08E-16 2.00E-12 S.OOE-13 1.62E-14 4.00E-12 l.OOE-12
11/14/1988 3.94E-15 S.OOE-12 1.25E-12 2.12E-15 8.00E-14 2.00E-14 1,01E-15 2,00E-12 S,OOE-13 2.47E-14 4,00E-12 l.OOE-12
2/13/1989 1.99E-15 5,00E-12 1.2SE·12 5.73E-16 S.OOE-14 2.00E-14 5.99E-16 2.00E-12 S.OOE-13 3.23E-14 4.00E-12 l.OOE-12
5/15/1989 1.70E-15 5,00E-12 1.25E-12 6.32E-16 S.OOE-14 2.00E-14 5.86E-16 2,00E-12 S.OOE-13 6.16E-15 4.00E-12 l.OOE-12
8/14/1989 2.31E-15 5.00E-12 1.25E-12 2.31E-16 S.OOE-14 2.00E-14 1.77E-16 2.00E-12 S.OOE-13 7.65E-15 4.00E-12 l.OOE-12
11/13/1989 4.72E·15 S.OOE-12 1.2SE-12 1.71E-15 S.OOE-14 2.00E-14 1.52E-15 2.00E-12 5.00E-13 1.89E-14 4.00E-12 l.OOE-12
2/12/1990 3.44E-16 S.OOE-12 1.25E-12 8.39E-16 S.OOE-14 2,00E-14 8.31E-16 2.00E-12 5.00E-13 2.57E-14 4.00E-12 l.OOE-12
5/14/1990 3,03E-15 S.OOE-12 1.2SE-12 1.47E-15 B.OOE-14 2.00E-14 1.04E-15 2.00E-12 S.OOE-13 1.79E-14 4.00E-12 l.OOE-12
8]13/1990 1.64E-15 5.00E-12 1.2SE·12 1.49E-15 S.OOE-14 2.00E-14 3.34E-16 2.00E-12 S,OOE-13 8,27E-15 4.00E-12 l.OOE-12
11/12/1990 1.48E-15 S,OOE-12 1.25E·12 7.SOE-16 S.OOE-14 2.00E-14 5.80E-16 2.00E-12 S.OOE-13 2.16E-14 4.00E-12 1.00E-12
2/11/1991 1.90E-16 S.OOE-12 1.25E-12 3.48E-17 S.OOE-14 2.00E-14 7.91E-17 2.00E-12 S.OOE-13 3.79E-14 4.00E-12 l.OOE-12
5/13/1991 3.42E-16 S.OOE-12 1.25E-12 1.34E-15 S.OOE-14 2.00E-14 7.39E-16 2.00E-12 S.OOE-13 1.46E-14 4 OOE-12 l.OOE-12
8/12/1991 2.77E-16 S.OOE-12 1.25E·12 4.17E-17 8 OOE-14 2.00E-14 1.45E-16 2.00E-12 S.OOE-13 1.80E-14 4 OOE-12 l.OOE-12
11/11/1991 6.65E-17 5.00E-12 1.2SE·12 9.13E-17 8.00E-14 2.00E-14 2.77E-17 2.00E-12 5.00E-13 1.06E-14 4.00E-12 l.OOE-12
2/10/1992 1,94E-16 ,S.OOE-12 1.25E-12 4.28E-17 8.00E-14 2.00E-14 4.08E-17 2.00E-12 5.00E-13 3.51E-14 4.00E-12 l.OOE-12
5/11/1992 2.54E-16 6.00E-12 1.25E-12 6.49E-16 S.OOE-14 2,00E-14 6.86E-17 2.00E-12 S.OOE-13 1.38E-14 4.00E-12 1,00E-12
8/10/1992 1.73E-16 5.00E-12 1.25E-12 1.55E-16 8.00E-14 2.00E-14 1.20E-16 2.00E-12 5.00E-13 l.S3E-14 4.00E-12 1,00E-12
11/9/1992 1,56E-16 S.OOE-12 1.2SE-12 3.19E-17 B.OOE-14 2.00E-14 4.90E-18 ,2.00E-12 S.OOE-13 1.86E-14 4 OOE-12 1.00E·12
2/9/1993 2.10E-16 5.00E-12 1.25E-12 8.00E-14 2.00E-14 3.89E-17 l.OOE-12 5.00E-13 2.52E-14 4.00E-12 1.00E-12
5/10/1993 1.00E-16 5,00E-12 1.25E-12 4.11E-17 8.00E-14 2.00E-14 6.43E-17 2.00E-12 S.OOE-13 1.26E-14 4.00E-12 l.OOE-12
8/10{1993 2.30E-16 5.00E-12 1.25E·12 6.00E-17 8.00E-14 2.00E-14 6.43E-17 .Z.OOE-12 S.OOE-13 1.60E-14 4.00E-12 l.OOE-12
11/8/1993 5.00E-12 1.25E-12 8.00E·14 l,OOE-14 O.OOE+OO 2.00E-12 5.00E-13 1.57E-14 4.00E-12 1.00E-12
2/7/1994 1.82E-16 5.00E-12 1,2SE-12 S.OOE-18 8.00E-14 .2.00E-14 4.30E-17 2.00E-12 5.00E-13 2.59E-14 4.00E-12 l.OOE-12
5/9/1994 3.60E-16 5.00E-12 1.25E·12 2.70E-16 8.00E-14 .Z.OOE-14 2.87E-16 2.00E-12 S.OOE-13 1.60E-14 4.00E-12 l.OOE-12
8/9/1994 4.04E-16 5.00E-12 '1.25E-12 2.70E-16 8 OOE-14 2.00E-14 2.94E-16 2.00E-12 5.00E-13 2.00E-15 4.00E-12 l.OOE-12
11/7/1994 9.18E-17 5.00E-12 1.25E-12 3.60E-16 B.OOE-14 2.00E-14 2.91E-16 2.00E-12 5.00E-13 2.00E-15 4.00E-12 l.OOE-12 -
Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-1U Effluent Concentration Limit= •2E-14 uCi/ml BHV-lT Effluent Concentration Limit = !lE-13 uCifml BHV-1R Effluent Concentration Limit= 6E-13 uCi/ml BHV-1PB
ALARAGoal = IZ.25E-14 uCi/ml ALARAGoal = SE-13 uCij ml ALARA Goal= :Z.25E-13 uCi/ml ALARA Goal= l.SE-13 uCi/ml
Pre l994•MPC Umll = SE-12 uCi/ml Pre 1994 MPC Limit= BE-14 uCi/ml Pre 1994 MPC Limit-:ZE-12 uCi/ml Pte 1.!!94 MPC limit"' 4E-12 uCi/ml
Pre 1994 A LARA GOAL = 1.25E-12 uCi/ml Pre 1994 A LARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL= lE-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
2/7/1995 1.77E-16 '9.00E-14 2.25E-14 9.70E-17 2.00E-14 .S.OOE-15 9.70E-17 9.00E-13 2.25E-13 8.60E-15 6.00E-13 1.50E-13
5/9/1995 9.40E-17 9.00E-14 2.25E-14 5.36E-16 2.00E-14 5.00E-15 1.60E-15 S.OOE-13 2.25E-13 3.84E-15 6.00E-13 1.50E·13
8/9/1995 2.70E-16 9,00E-14 2.25E-14 1,60E-16 2.00E-14 S.OOE-15 ~.76E-16 9,00E-13 2.25E-13 .3.76E-15 6.00E-13 1.50E-13
11/11/1995 4.80E-15 9.00E-14 2.25E-14 6.41E-16 2.00E-14 6.00E-15 8.93E-16 9.00E-13 2.25E-13 5.20E-15 6.00E-13 1.50E-13
2/5/1996 5.34E-15 9.00E-14 2.25E-14 2.30E-15 2.00E-14 S.OOE-15 1.30E-15 9.00E-13 2.25E-13 4.20E-15 6.00E-13 1.50E-13
:S/6/1996 5.11E-16 9.00E-14 2.25E-14 3.06E-16 2.00E-14 S.OOE-15 1.40E-16 fJ.OOE-13 2.25E-13 7.03E-15 6.00E-13 i.SOE-13
8/5/1996 5.99E-16 9.00E-14 2,25E-14 1.55E-15 2.00E-14 .S.OOE-15 2.03E-16 9.00E-13 2.25E-13 5.94E-15 6.00E-13 1.50E-13
11/6/1996 B.38E-16 9.00E-14 2.25E-14 5.45E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E·13 1.22E-14 6.00E-13 1.50E-13
2/6/1997 1,00E-16 9.00E-14 2..25E-14 1.25E-16 2.00E-14 S.OOE-15 1.28E-16 9.00E-13 2.25E-13 5.68E-15 6.00E-13 .1.50E-13
'?/5/1997 1.09E-16 9,00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9,00E-13 2,25E-13 4.39E-15 6.00E-13 1.50E-13
S/11L1997 2.88E-16 9.00E-14 2.25E-14 3.83E-16 2.00E-14 S,OOE-15 1.82E-16 9,00E-13 2.25E-13 5.29E-15 6.00E-13 1.50E-13
1/S/1~ 3.24E-16 9.00E-14 2.25E-14 3.47E-16 2.00E-14 S.OOE-15 1,19E-16 9,00E-13 2.25E-13 4.73E-15 6.00E-13 1.50E-13
4/28/1998 4.75E-16 9.00E-14 2.25E-14 6.73E-16 2.00E-14 5.00E-15 5.69E-16 9.00E-13 225E-13 5.94E-15 6.00E-13 1.SOE-13
7/31/1998 8.84E-16 9.00E-14 2.25E-14 1.93E-15 2.00E-14 5.00E-15 1.43E-15 9.00E-13 2.25E-13 5.22E-15 6.00E-13 1.50E-13
9/28/1998 2.81E-16 9.00E-14 2"25E-14 2.89E-16 2.00E-14 S.OOE-15 1.80E-16 9.00E-13 2.25E-13 4.64E-15 6.00E-13 l.SOE-13
12/28/1998 8.08E-16 9.00E-14 2.25E-14 4.93E-16 2.00E-14 S,OOE-15 S.OlE-16 9.00E-13 2.25E-13 1.06E-14 6.00E-13 l.SOE-13
3/29/JSS9 2.06E-16 9.00E-14 2.25E-14 .2.06E-16 2.00E-14 S.OOE-15 1.42E-16 9.00E-13 2.25E-13 6,69E-15 6.00E-13 1.50E-13
7/3/1999 5.31E-16 9.00E-14 2.25E-14 .2.47E-16 2.00E-14 S.OOE-15 2,23E-16 9.00E-13 2.25E-13 6.44E-15 6.00E-13 1.50E-13
9/27/1999 8.98E-16 9.00E-14 2.25E-14 3.90E-16 2.00E-14 5.00E-15 2.96E-16 9.00E-13 2.25E-13 7.29E-15 6.00E-13 1.50E-13
12/28/1999 1.48E-15 9.00E-14 2.25E-14 6.00E-16 2.00E-14 5.00E-15 5,57E-16 9.00E-13 2.25E-13 6.19E-15 6.00E-13 1.50E-13
3/27/2000 1.00E-16 9.00E-14 2.25E-14 1.06E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6,23E-15 6.00E-13 1.50E-13
6/26/2000 3.47E-16 9.00E-14 2.25E-14 3.46E-16 2.00E-14 5.00E-15 3.62E-16 9.00E-13 2.25E-13 4.50E-15 6.00E-13 1.50E-13
9/26/2000 2.51E-16 9.00E-14 2.25E-14 1.78E-16 2.00E-14 5.00E-15 3.25E-16 9.00E-13 2.2SE-13 8.55E-15 6,00E-13 1.50E-13
12/26/2000 1.00E-16 9.00E-14 2.25E-14 1.42E-16 2.00E-14 5,00E-15 1.31E-16 9.00E-13 2.25E-13 7.77E-15 6.00E-13 1.50E-13
3/26/2001 3.10E-16 S.OOE-14 2.25E-14 l.OOE-15 2.00E-14 5.00E-15 l.OOE-15 9.00E-13 2.25E-13 7.19E-15 6.00E-13 1.50E-13
7/29/2001 1.52E-16 9.00E-14 2.25E-14 1.44E-16 2.00E-14 5.00E-15 1.77E-16 9.00E-13 2.25E-13 7.21E-15 6.00E-13 1.50E-13
9/24/2001 1,03E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.09E-15 6.00E-13 1.50E-13
12/31/2001 1.00E-16 9.00E-14 2.25E-14 LOOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.39E-15 6.00E-13 1.50E-13
4/1/2002 2.05E-16 9.00E-14 2.25E-14 2.44E-16 2.00E-14 5.00E-15 2,29E-16 !J.OOE-13 2,25E-13 8.15E-15 6,00E-13 1.50E-13
7/1/2002 3.55E-16 9.00E-14 2.25E-14 4.85E-16 2.00E-14 5.00E-15 1.06E-16 9.00E-13 2.25E-13 7.65E-15 6.00E-13 1.50E-13
9/30/2002 1.17E-16 ~.OOE-14 2.25E-14 1.61E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 .3.68E-15 6.00E-13 1.50E-13
12/30/2002 1.00E-16 9.00E-14 2.25E-14 1.03E-16 2,00E-14 5.00E-15 l.OOE-16 9,00E-13 2.25E-13 9.46E-15 6.00E-13 1.50E-13
Y31/2003 1.20E-16 9.00E-14 2.25E-14 1.12E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 4.68E-15 6.00E-13 1.50E-13
6/30/2003 2.18E-16 9.00E-14 2.25E-14 3.40E·16 2.00E-14 5.00E-15 1.67E-16 9.00E-13 2.25E-13 5.96E-15 6.00E-13 1.50E-13
9/29/2003 1,00E-16 9.00E-14 225E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 g.OOE-13 2,25E-13 728E-15 6.00E-13 1.50E-13
12/29/2003 l.OOE-16 9.00E-14 2.25E-14 2.54E-16 2.00E-14 S.OOE-15 3.35E-16 ~.OOE-13 2.25E-13 6.25E-15 6.00E-13 1.50E-13
3}29/2004 l.OOE-16 9.00E-14 2,25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.54E-14 6.00E-13 1.50E-13
6/27/2004 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2 OOE-14 ?.OOE-15 l.OOE-16 g.OOE-13 2.25E-13 3.04E-15 6.00E-13 1,50E-13
9/27/2004 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.05E-14 6.00E-13 l.SOE-13
12/27/2004 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9,00E-13 2.25E-13 1.59E-14 6.00E-13 1.50E-13
3/28/2005 l.OOE-16 9,00E-14 2.25E-14 l.OOE-16 2,00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.42E-15 6.00E-13 1.50E-13
6}29/2005 l.OOE-16 9,00E-14 2.25E-14 1.30E-16 2.00E-14 .S.OOE-15 1.20E-16 9.00E-13 2.25E-13 7.94E-15 6.00E-13 1.50E-13
9/26/2005 l.OOE-16 9.00E-14 2.25E-14 2.56E-16 2.00E-14 5.00E-15 2.42E-16 9.00E-13 2.25E-13 1.22E-14 6.00E-13 1.50E-13
1/3/2006 2.13E-16 9.00E-14 2.25E-14 1.04E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 3J3E-14 6.00E-13 1.50E-13
4/3/2006 1.62E-16 9.00E-14 2,25E-14 1.86E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2,25E-13 8.36E-15 6.00E-13 1.50E-13
7/3/2006 1.86E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 9.77E-15 6.00E-13 1.50E-13
10/2/2006 1,00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.-25E-13 1.30E-14 6.00E-13 1.50E-13
1/1/2007 l.OOE-16 9,00E-14 2.25E-14 1.47E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.17E-14 6.00E-13 1.50E-13
4/2/2007 2.23E-16 9,00E-14 2.25E-14 1.63E-16 ,2,00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 1.65E-14 6.00E-13 1.50E-13
7/2/2007 3.35E-16 9,00E-14 2.25E-14 1.34E-16 :Z.OOE-14 S.OOE-15 1.36E-16 9.00E-13 2.25E-13 1.78E-14 6.00E-13 1,50E-13
9/30/2007 1.15E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 7.68E-15 6.00E-13 1.50E-13
12/31/2007 l.OOE-16 9.00E-14 ,2,25E-14 1.93E-16 2.00E-14 S.OOE-15 1,00E-16 9,00E-13 2,25E-13 l.31E·14 6.00E·13 1.50E·13
3/31/2008 1.14E-16 9.00E-14 2.25E-14 1.13E-16 2.00E-14 5.00E-15 1.00E-16 9,00E·13 2,25E-13 6.44E·15 6.00E-13 1.50E-13
6/30/2008 7.09E-16 9,00E-14 2.25E-14 3.83E-16 2.00E-14 5.00E-15 2.27E-16 9.00E-13 2.25E-13 6.52E-15 6.00E-13 1.50E-13
Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-1U Effluent Concentration Limit= ZE-14 uCi/ml BHV-lT Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration limit -6E-13 uCi/ml BHV-1PB
ALARAGoal-•Z.ZSE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal -Z.ZSE-13 uCi/ml ALARA Goal= l.SE-13 uCi/ml
Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC limit= SE-14 uCi/ml Pre 1994 MPC limit = 2E-12 uCi/ml Pre 1994 MPC Limit= IIE-1ZuCVml
Pre 1994 A LARA GOAL= l.ZSE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 A LARA GOAL-1E-1Z uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
9/30/2008 7.69E-16 9.00E-14 2.25E-14 2.94E-16 ,2.00E-14 5.00E-15 1.90E-16 9.00E-13 2.25E-13 7.64E-15 6.00E-13 1.50E-13
12.131/2008 1.21E-15 9.00E-14 2.25E-14 4.76E-16 2.00E-14 5,00E·15 3.34E-16 9.00E-13 2.25E-13 1.16E-14 6.00E-13 1.50E-13
3/15/2009 2.14E-15 9.00E-14 2.25E-14 1.02E-15 2.00E-14 5.00E-15 l.OOE-15 9.00E-13 2.25E-13 4.44E-15 6.00E-13 1.50E-13
8l l5/2.009 5.97E-17 9,00E-14 2.25E-14 2.35E-16 2,00E-14 S.OOE-15 2.18E-16 9,00E-13 2.25E-13 5.13E-15 6.00E-13 1,50E-13
9/15/2009 9.55E-16 9.00E-14 2.25E-14 1.71E-16 .2.00E-14 5.00E-15 9.87E-17 9.00E-13 2.25E-13 9.47E-15 G.OOE-13 1.50E-13
12/15/2009 1.24E-15 9.00E-14 2.25E-14 9.25E-17 2.00E-14 S.OOE-15 5.60E-17 9.00E-13 2.25E-13 5.95E-15 G,OOE-13 1.50E-13
3/31/2010 1.97E-15 9.00E-14 2.25E-14 2.15E-16 Z.OOE-14 5.00E-15 3.27E-16 9.00E-13 2.25E-13 l.OOE-14 6.00E-13 1.50E-13
6/30/2010 1.58E-15 9.00E-14 2.25E-14 4.71E-16 2.00E-14 5.00E-15 7.70E-16 9.00E-13 ,2.25E-13 4,07E-15 6.00E-13 1.SOE-13
9/3o/2010 8.42E-16 9.00E-14 2.25E-14 2,80E-16 2.00E-14 5.00E-15 1.31E-16 9.00E-13 2.25E-13 6.80E-15 6.00E-13 1.SOE-13
12/31/2010 1.27E-15 9.00E-14 2.25E-14 2.32E-16 2.00E-14 5.00E-15 2.30E-16 g.OOE-13 2.25E-13 1.27E-14 G.OOE-13 1.50E-13
4/4/2011 9.01E-16 9.00E-14 2.25E-14 1.90E-16 2.00E-14 5.00E-15 3.64E-16 9.00E-13 2,25E-13 1.09E-14 6.00E-13 1.50E-13
7/4/2011 1.59E-15 9.00E-14 2.25E-14 5,31E-16 2.00E-14 ~.OOE-15 4.99E-16 9.00E-13 2.25E-13 S.38E-15 6.00E-13 1,50E-13
10/3/2011 2.92E-16 9.00E-14 2.25E-14 L17E·16 2.00E-14 S.OOE-15 6.76E-17 9.00E·13 '2.25E-13 1.14E-14 6.00E-13 1.50E-13
1/3/2012 6.73E-16 9.00E-14 2.25E-14 1.19E-16 2.00E-14 S.OOE-15 8.58E-17 9.00E-13 2.25E-13 1.73E-14 6.00E-13 l.SOE-13
4/3/2012 7.87E-16 9.00E-14 2.25E-14 2.64E-16 2.00E-14 5,00E-15 3.95E-16 9.00E-13 2.25E-13 1.25E-14 G.OOE-13 1.50E-13
7/2/2012 1.86E-15 9,00E-14 2.25E-14 8.33E-16 2.00E-14 5.00E-15 9.85E-16 9,00E-13 2.25E-13 9.55E-15 G.OOE-13 1.50E-13
10/1/2012 l.OGE-15 9.00E-14 2.25E-14 2.11E-16 2.00E-14 5.00E-15 2.34E-16 9.00E-13 2,25E-13 1,13E-14 G.OOE-13 1.50E-13
12/31/2012 6.86E-16 9.00E-14 2.25E-14 1.27E-16 .Z.OOE-14 S.OOE-15 1.38E-16 9.00E-13 2.25E-13 1.54E-14 6.00E-13 1.50E-13
3/25/2013 9.91E-16 9.00E-14 .2.25E-14 1.86E-16 Z.OOE-14 5.00E-15 2.04E-16 9.00E-13 2.25E-13 1.82E-14 G.OOE-13 l.SOE-13
7/2/2013 1.46E-16 9.00E-14 2.25E-14 3.34E-16 Z.OOE-14 5.00E·15 3.91E-16 9,00E-13 .2.25E-13 5.78E-15 6.00E-13 1.50E-13 -----
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6o-das
so-das
Lo-das
go-d as
so-das
vo-das
8o-das
Go-das
w-das
oo-das
66-das
B6·das
L6·das
95-das
95-das
v6-das
86-das
G6·das
~5-das
06-das
6B·das
gg-das
Le-das
gg-das
gg-das
pg-das
8e-das
GB-das
~g-das
tn
s::::: 0 ·~ -s::::: Q)
(,)
s:::::
0 (.)
0 ,....
C\1 I
"C ca Q)
...J ,....
:> ::I: m
,.... ,....
I w 0 ~
C\1 C') ,....
uJ I w 0 0 ~ ~ ,....
~ J.
~
• lit
~
~
!"'f-. I-+-
~ ~ .,.:::;
• ==-•
~
• ~ ..
)I •
;,I
~
:tc!.
.:~ ~-;;;~
:«:..t'V .,___
"r.. ~ ~ t_ ==-
-;I
!.
~~ J .::::::: ---.
~F: :.,_j.
~
"<:t ,....
I w
0 0
(a1e::rs oo1)
L{) CD ,.... ,....
I I w w 0 0 ~ ~ ,....
-
-
.
-
-
I'-,....
I w 0 ~
G~-das
~~-des
o~-das
6o-das
so-das
Lo-des
go-des
so-das
vo-das
8o-das
Go-des
~o-des
oo-das
55-das
95-das
L6-das
95-das
95-das
175-das
86-das
G6-das
~5-das
05-das
6s-das
ss-das
Ls-das
gg-das
gg-das
vs-das
8s-das
Gs-das
~s-das
TAB2
BHV-2 AIR SAMPLING GRAPHS AND DATA TABLE
Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-2U ~!fluent Concentration Limit= lf-14 uCI/ml BHV-2T Effluent Concentration Limit -9E-13 uCi/ml BHV-2R Effluent Concentration Limit = 6E-13 uCi/ml BHV-2PB
ALARA Goal= 2.25E-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal-2.25E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml
Pre 1994 MPC Limit= SH2u-cl/)111 pre 1994 MPC Limit= SE-14 uCi/ml Pre 1994 MPC Limit = ZE-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml
Pre 1994 ALARA GOAL = l .ZSE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 A LARA GOAL-1E-12 uCi/ml
Cone ~FC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
9{28/1981 1.39E-15 S.OOE-12 1.25E-12 3.69E-16 B.OOE-14 2.00E-14 5.92E-16 2.00E-12 5.00E-13 1.67E-14 4.00E-12 l.OOE-12
H/t4/19Sl 4.62E-16 S.OOE-12 1.25E-12 8.03E-16 B.OOE-14 2.00E-14 3.62E-16 2.00E-12 S.OOE-13 1.33E-14 4.00E-12 l.OOE-12
3/29}1982 7.07E-16 S.OOE-12 1.25E-12 l.lOE-15 B.OOE-14 2.00E-14 7.27E-16 2.00E-12 S.OOE-13 1.52E·14 4.00E-12 l.OOE-12
6/30/1982 8.84E-16 5.00E-12 1.25E-12 7.73E-16 8.00E-14 2.00E-14 4.78E-16 2.00E-12 ~.OOE-13 1.98E-14 4.00E-12 l.OOE-12
9/27/1982 1.23E-15 5.00E-12 1.25E-12 3.60E-16 8,00E-14 2.00E-14 8,73E-16 2.00E-12 S.OOE-13 2.35E·14 4.00E-12 l.OOE-12
l/3/1983 2.64E-15 5.00E-12 1.25E-12 2.55E-16 8.00E-14 2.00E-14 1.98E-16 2.00E-12 S.OOE-13 2.85E-14 4.00E-12 l.OOE-12
.fl/"'l-mB3 2.14E-16 5.00E-12 1.25E-12 1.02E-16 8.00E-14 2.00E-14 1.57E-16 2.00E-12 S.OOE-13 M8E-14 4.00E-12 1.00E-12
6/30/1.983 2.85E-16 S.OOE-12 1.25E-12 2.06E-16 B.OOE-14 Z,OOE-14 2.24E-16 2,00E-12 S.OOE-13 1.79E·14 4.00E-12 1.00~12
10/3/1983 2.70E-16 5.00E-12 1.25E-12 3.36E-16 B.OOE-14 2.00E-14 4.37E-16 2.00E-12 5.00E-13 1.78E-14 4.00E-12 l.OOE-12 i
1/3/1984 2.78E-15 S.OOE-12 1.25E-12 1.20E-16 S.OOE-14 2.00E-14 6,64E-17 2.00E-12 5.00E-13 9.14E·15 4.00E-12 l.OOE-12 !
4/l/1984 4.28E-16 S.OOE-12 1.25E-12 1.75E-16 ll.OOE-14 2.00E-14 4.57E-17 2.00E-12 5.00E-13 3.55E-14 4,00E-12 l.OOE-12 '
7/2}1984 2.78E-15 5.00E-12 1.25E-12 8.12E-16 8.00E-14 2.00E-14 1,98E-16 2 OOE-12 5.00E-13 1.68E·14 4.00E-12 l.OOE-12
10}1/1984 2.69E-16 5.00E-12 1.25E-12 2.66E-17 B.OOE-14 2.00E-14 O.OOE+OO 2.00E-12 li.OOE-13 1,77E·14 4.00E-12 1,00E-12
1/2/1985 2.15E-16 5.00E-12 1.25E-12 7,55E-16 B.OOE-14 .2.00E-14 2.87E-16 2.00E-12 S.OOE-13 3.19E-14 4.00E-12 l.OOE-12
4/1/1985 l.OOE-16 5.00E-12 1.25E-12 L67E-16 8.00E-14 2.00E-14 6.75E-17 2.00E-12 S.OOE-13 7.56E-15 4.00E-12 l.OOE-12
7/1/1985 3.70E-17 5.00E-12 1.25E-12 9.00E-16 8.00E-14 2.00E-14 4.90E-17 2.00E-12 S.OOE-13 1.31E-14 4.00E-12 l .OOE-12
9/30/1985 9.32E-17 S,OOE-12 1.25E-12 2.18E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 S.OOE-13 3.64E-15 4.00E-12 l.OOE-12
1/2/-1986 1.00E-16 5.00E-12 1.25E-12 2.16E-16 B.OOE-14 2.00E-14 2.15E-17 2.00E-12 S.OOE-13 3.04E-16 4.00E-12 l.OOE-12 ,
4/l/1986 1.31E-15 5.00E-12 1.25E-12 l.SOE-16 B.OOE-14 2.00E-14 3.71E-16 2.00E-12 5,00E-13 2.90E-15 4.00E-12 l.OOE-12 1
6/30/J!j86-2.23E-16 5.00E-12 1.25E-12 1,32E-16 S.OOE-14 2.00E-14 7.09E-17 2.00E-12 S.OOE-13 2.53E-14 4,00E-12 l.OOE-12
10/27/1986 6.41E-16 S.OOE-12 L25E-12 1.74E-16 S.OOE-14 2.00E-14 3.67E-16 2.00E-12 5.00E-13 1.04E-14 4.00E-12 l.OOE-12
12/·15/1986 3.56E-16 S.OOE-12 1.25E-12 1.00E-16 S.OOE-14 2.00E-14 1.05E-16 2.00E-12 S.OOE-13 7.81E-15 4.00E-12 1.00E-12
3/16/1987 5.31E-16 S.OOE-12 1.25E-12 1.30E-16 8.00E-14 2.00E-14 7.74E-17 2.00E-12 5.00E-13 3.80E-14 4.00E-12 l.OOE-12
S/l.l/1951 4.06E-16 S.OOE-12 125E-12 6.63E-17 B.OOE-14 2.00E-14 1.34E-16 2.00E-12 'S.OOE-13 1.10E-14 4.00E-12 l.OOE-12
9/9/1987 2.74E-16 5,00E-12 1.25E-12 2.38E-16 8.00E-14 2,00E-14 1.38E-16 2.00E-12 S.OOE-13 1.04E·14 4.00E-12 1.00E-12
11/2/1987 3.73E-16 5.00E-12 1.25E-12 3.11E-16 8,00E-14 2.00E-14 1.83E-16 l.OOE-12 S.OOE-13 1.17E-14 4.00E-12 l.OOE-12 I
l/1.&/19l!8 2.78E-15 5.00E-12 1.25E-12 2.31E-17 8,00E-14 2.00E-14 1.20E-16 2.00E-12 S.OOE-13 3.55E-14 4.00E-12 l.OOE-12
5/l.S/1~83 4.63E-16 5.00E-12 1.25E-12 1.49E-16 8.00E-14 2.00E-14 2.30E-16 2.00E-12 5.00E-13 1.18E-14 4.00E·12 l.OOE-12
8!15/.'1.988 8.06E-16 S.OOE-12 1.25E-12 8,69E-16 B.OOE-14 2.00E-14 1.80E-16 2.00E-12 S.OOE-13 1.42E-14 4.00E-12 l.OOE-12
ll/14/1983 4.34E-16 5.00E-12 ~.25E-12 6.76E-16 S.OOE-14 2.00E-14 1.57E-16 2.00E-12 5,00E-13 2,25E-14 4.00E-12 l.OOE-12
2/l3/lS89 5.80E-16 5.00E-12 1.25E-12 2.85E-16 B.OOE-14 2.00E-14 1.55E-16 2.00E-12 5.00E-13 2.80E-14 4.00E-12 l.OOE-12
5/15/1989 5.06E-16 5.00E-12 1.25E-12 2.28E-16 S.OOE-14 2.00E-14 1.63E-16 2.00E-12 S.OOE-13 6,05E-15 4.00E·12 1.00E-12
8/14}1989 4.71E-16 S.OOE-12 1.25E-12 9.60E-16 S.OOE-14 2.00E-14 1.26E-15 2,00E-12 S.OOE-13 6.65E-15 4.00E-12 1 OOE-12 I
11/13/1989 1.14E-15 S.OOE-12 1.25E-12 4.08E-16 B.OOE-14 2.00E-14 4.18E-16 2.00E-12 5.00E-13 1.59E-14 4.00E·12 1.00E-12
2/12/1990 1.09E-15 S.OOE-12 1.25E-12 3.25E-16 S,OOE-14 2.00E-14 3.74E-16 2.00E-12 5.00E-13 1.98E-14 4.00E-12 1.00E-12
5/14/1990 9.32E-16 S.OOE-12 1.2SE-12 5.27E-16 B.OOE-14 2.00E-14 3.97E-16 .Z.OOE-12 l;.OOE-13 1.69E-14 4.00E·12 l.OOE-12
8/13/1990 1.66E-16 5.00E-12 1.25E-12 5.49E-16 8.00E-14 2.00E-14 4.75E-17 Z.OOE-12 S.OOE-13 1.27E-15 4.00E-12 1.00E-12
11/12/1990 6.05E-16 5.00E-12 1.25E-12 2.64E-16 8.00E-14 2.00E-14 1.93E-16 Z.OOE-12 S.OOE-13 Z.25E-14 4.00E-12 l.OOE-12
2/11/1991 8.72E-17 S.OOE-12 1.25E-12 7.00E-18 8.00E-14 2.00E-14 3.33E-17 Z.OOE-12 S.OOE-13 3.49E-14 4.00E·l2 1.00E-12
5/13/1991 1.16E-16 S,OOE-12 1.25E-12 3.86E-16 B.OOE-14 2.00E-14 2.80E-16 2.00E-12 S.OOE-13 1.50E-14 4.00E·12 l.OOE-12
S/U/1991 9,02E-17 5.00E-12 1.25E-12 8,82E-17 B.OOE-14 2.00E-14 7.65E-17 2.00E-12 S.OOE-13 1.58E·14 4.00E-12 l.OOE-12
i l/U/1991• 4.81E-17 S.OOE-12 .1.25E-12 3.82E-17 B.OOE-14 2,00E-14 2.54E-17 2.00E-12 5.00E-13 1.45E-14 II.OOE-12 1.00E-12
2/l0/J!j92 1.54E-16 6.00E-12 1.25E-12 6.82E·17 8.00E-14 2,00E-14 1.40E-17 2.00E-12 5.00E-13 3.41E-14 4.00E-12 l.OOE-12
Sil'l/1992 2,38E-16 S.OOE-12 1.25E-12 7.63E-17 8,00E-14 2.00E-14 3.07E-17 2.00E-12 5.00E-13 1,27E-14 4.00E-12 l.OOE-12
8/10/1992 1.01E-16 S.OOE-12 1.25E-12 7.07E-17 B.OOE-14 2.00E-14 2.80E·17 2.00E-12 S.OOE-13 1.41E-14 4.00E-12 l.OOE-12
11/9/1992 5.20E-17 5.00E-12 1.25E-12 3.65E-17 8.00E-14 2.00E-14 1.78E-17 2,00E-12 S.OOE-13 1,71E-14 4.00E-12 1 OOE-12
2/9/1993 2.39E-16 5.00E-12 1.25E-12 2.97E-17 8,00E-14 2.00E-14 G.31E-17 2.00E-12 S.OOE-13 .3.41E-14 4.00E-12 l.OOE-12
5/10/1993 l.OOE-16 5.00E-12 1.25E-12 7.11E-17 B.OOE-14 .2.00E-14 3,19E-17 2.00E-12 S.OOE-13 1.34E-14 4.00E-12 1.00E-12
8/10/1993 1.90E-16 5,00E-12 1.25E-12 1,00E-16 8,00E-14 ,2.00E-14 l.OOE-16 Z.OOE-12 S.OOE-13 l.SOE-14 4.00E-12 l.OOE-12
11/8/1993 1.00E-16 S.OOE-12 1.25E-12 l.OOE-16 B.OOE-14 z,OOE-14 l.OOE-16 2.00E-12 s.OOE-13 1.49E-14 4.00E·12 l.OOE-12
2/7/1994 2.23E-16 S.OOE-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 184E-16 2.00E-12 5.00E-13 2.19E·14 4.00E-12 1.00E-12
S/9/l!YYJ 2.16E-16 S.OOE-12 1.25E-12 7.20E-17 S.OOE-14 2.00E-14 9.89E-17 2.00E-12 5.00E-13 1.37E-14 II,OOE-12 1.00E-12
8/9/1.99~ 9.29E-17 S.OOE-12 1.25E-12 2.96E-16 S.OOE-14 2.00E-14 3.04E-16 2.00E-12 5.00E-13 l.OOE-16 4.00E·12 1.00E-12
U/7jl<J9~--9.21E-17 S.OOE-12 1.25E-12 2.35E-16 8.00£-14 2.00E-14 l.OOE-16 2.00E-12 5,00E-13 l.OOE-16 4.00E·12 1.00E-12
Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-ZU Effluent Concentration Limit-ZE-14 uCi/ml BHV-2T Effluent Concentration Limit = 9E-13 uCi/ml BHV-ZR Effluent Concentration Limit-6E-13 uCi/ml BHV-2PB
ALARA Goal= 2.25E-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal-2.25E-13 uCi/ml ALARA Goal-1.5E-13 uCi/ml
Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC Limit= BE-14 uCi/ml Prec1994 MPC Unilt-= ZE-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml
Pre 1994 ALARA GOAL= i .ZSE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL= 1E-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
2/7/1995 1.18E-16 g.OOE-14 2.25E-14 9.70E-17 2.00E-14 5.00E-15 9.70E-17 9.00E-13 2.25E-13 7-42E-15 6.00E-13 1.50E-13
5/9/1995 9.40E-17 9.00E-14 2.25E-14 1,20E-16 2.00E-14 5.00E-15 3.SOE-16 9.00E-13 2,25E-13 3.90E-15 6.00E-13 1.50E-13
8/9/1995 8.90E-17 9.00E-14 2.25E-14 9.67E-17 2.00E-14 5.00E-15 1.35E-16 9.00E-13 2.25E-13 2,38E-16 6.00E-13 1.50E-13
11{11/1995 2.83E-15 9.00E-14 2.25E-14 4.09E-16 2.00E-14 5.00E-15 5.23E-16 9.00E-13 .2,25E-13 p.77E-15 6.00E-13 150E-13
2/5/1996 1.75E-15 9.00E-14 2.25E-14 8,66E-16 2.00E-14 5.00E-15 4.86E-16 9.00E-13 7.25E-13 3.SOE-15 6.00E-13 l.50E-13
5/6/1996 1.40E-16 9.00E-14 2,25E-14 1.15E-16 2,00E-14 5.00E-15 l.OOE-16 9.00E-13 Z.25E-13 p.85E-15 6,00E-13 1.50E-13
8/5/1996 1.43E-16 9.00E-14 2.25E-14 2.78E-16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 5.83E-15 6.00E-13 1.50E-13
11/6/1996 1.45E-16 9.00E-14 2 25E-14 1.57E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 .2.25E-13 1.19E-14 6.00E-13 1.50E-13
2/6/1997 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 5.84E-16 6.00E-13 1.50E-13
5/5/1997 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 g.OOE-13 2.25E-13 3.89E-15 6.00E-13 1.50E-13
8/11/1997 l.OOE-16 9.00E-14 2.25E-14 1.09E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.69E-15 6.00E-13 1.50E-13
1/5/1998 2.55E-16 9.00E-14 2.25E-14 1.07E-16 2.00E-14 5.00E-15 5.00E-17 9.00E-13 2.25E-13 5.11E-15 6.00E-13 1.50E-13
4/28/1998 1.20E-16 9.00E-14 2.25E-14 L71E-16 2,00E-14 5.00E-15 1.28E-16 9.00E-13 2.25E-13 6.40E-15 6,00E-13 1.50E-13
7/31/1998 1.47E-16 9.00E-14 2.25E-14 4.24E-16 2.00E-14 5.00E-15 3.39E-16 9.00E-13 2.25E-13 4.80E-15 6.00E-13 l.50E-13
9/28/1998 l.OOE-16 9,00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 4.26E-15 6.00E-13 1.50E-13
12/28/1998 2.54E-16 9.00E-14 2.25E-14 2.15E-16 2.00E-14 s.OOE-15 1.38E-16 9.00E-13 2.25E-13 6.88E-15 6.00E-13 1.50E-13
.3/29/1999 1.07E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.61E-15 6.00E-13 1.50E-13
7/3/1999 2,46E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.95E-15 6.00E-13 1.50E-13
fJ/27/1999 2,81E-16 9.00E-14 2.25E-14 1.41E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.35E-15 6.00E-13 l.50E-13
12/28/1999 5.20E-16 9.00E-14 2.25E-14 2.60E-16 2.00E-14 5.00E-15 2.01E-16 9.00E-13 225E-13 7.00E-15 6.00E-13 1.50E-13
.3/27/2000 1.00E-16 9.00E-14 2.25E-14 l.OOE-16 ;Z.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.12E-15 6.00E-13 1,50E-13
6/26/2000 1.10E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.16E-16 9.00E-13 2.25E-13 5.07E-15 6.00E-13 1.50E-13
9/26/2000 l.OOE-16 9.00E-14 2,25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.31E-15 6.00E-13 1.50E-13
12/26/2000 1.26E-16 9.00E-14 2.25E-14 i.OOE-16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2,25E-13 9.45E-15 6,00E-13 1.50E-13
3/26/2001 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 Z.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.95E-15 6,00E-13 1.50E-13
7/2/2001 l.OOE-16 ll.OOE-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.56E-15 6.00E-13 1.50E-13
9/2412001 l.OOE-16 IJ.OOE-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.16E-15 6.00E-13 1.50E-13
12/31/2001 l.OOE-16 9.00E-14 r25E-14 l.OOE-16 Z.OOE-14 5.00E-15 1,00E-16 9.00E-13 2.25E-13 2.20E-15 6.00E-13 1.50E-13
4/1/2002 l.OOE-16 f.l,OOE-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 9,95E-15 6.00E-13 1.50E-13
7/1/2002 1.25E-16 '9.00E-14 2.25E-14 1.43E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 8.25E-15 6.00E-13 1,50E-13
9/30/2002 1.00E-16 9.00E-14 2.25E-14 l.OOE-16 .Z.OOE-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 3.69E-15 6.00E-13 l.SOE-13
12/30/2002 1.00E-16 9.00E-14 2.25E-14 l.OOE-16 Z.OOE-14 5 OOE-15 l.OOE-16 9,00E-13 2.25E-13 6.91E-15 6.00E-13 150E-13
3/31/2003 1.00E-16 S.OOE-14 2.25E-14 l.OOE-16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 6.16E-15 6.00E-13 1.50E-13
6/30/2003 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2,25E-13 5,27E-15 6.00E-13 1.50E-13
9/29}2003 l.OOE-16 S.OOE-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.23E-15 6.00E-13 1.50E-13
12/29/2003 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.80E-15 6,00E-13 1.50E-13
3/29/2004 1.00E-16 :'l.OOE-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 2.04E-14 6,00E-13 1.50E-13
6/27/2004 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 3.09E-15 6.00E-13 1.50E-13
9/27/2004 l.OOE-16 9.00E-14 2.25E-14 1,00E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.73E-14 6.00E-13 1.50E-13
12/27/2004 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 ,2.25E-13 1.30E-14 6.00E-13 1.50E-13
3/28/2005 l.OOE-16 9.00E-14 2,25E-14 1,00E-16 2,00E-14 5.00E-15 l.OOE-16 9.00E-13 ,2,25E-13 8.88E-15 6.00E-13 1.50E-13
6/29/2005 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 1.25E-13 8.85E-15 6.00E-13 1.50E-13
9/26/2005 l.OOE-16 9.00E-14 2.25E-14 1.99E-16 2.00E-14 .~.OOE-15 1.44E-16 9.00E-13 2.25E-13 3.81E-14 6.00E-13 1.50E-13
1/3}2006 1.29E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 4.08E-16 !l.OOE-13 2.25E-13 6.58E-14 p,OOE-13 1.50E-13
4/3/2006 1.02E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.08E-14 Ei.OOE-13 1.50E-13
7/3/2006 l.OOE-16 9,00E-14 2.25E-14 l.QOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 i .lOE-14 6.00E-13 1.50E-13
10/2/2006 1.30E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 .S.OOE-15 1,00E-16 S.OOE-13 2.25E-13 1.68E-14 6.00E-13 1.50E-13
1/1/2007 1.24E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2,25E-13 1.38E-14 6.00E-13 1.50E-13
4/2/2007 1.40E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 S.OOE-13 2.25E-13 1.63E-14 6.00E-13 l.SOE-13
7/2/2007 1.04E-16 9.00E-14 2 25E-14 l.OOE-16 2.00E-14 S,OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.36E-14 6.00E-13 l.50E-13
9/30/2007 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 8.24E-15 6.00E-13 1.50E-13
12/31/2007 1.91E-16 9,00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1,00E-16 9.00E-13 2.25E-13 1.18E-14 6.00E-13 1,50E-13
3/30/2008 l.OOE-16 9,00E-14 2.25E-14 1,00E-16 2,00E-14 5.00E-15 1,00E-16 9,00E-13 2.25E-13 6.49E-15 p.OOE-13 1.50E-13
6/30/2008 1.29E-16 9.00E-14 2.25E-14 l.OOE-16 2,00E-14 5.00E-15 1.00E-16 9.00E-13 2 25E-13 4,82E-15 6.00E-13 L50E-13
Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-2U Effluent Concentration Limit = 2E-14 uCi/ml BHV-2T Effluent Concentration Limit= 9E-13 uC[/ml BHV-2R Effluent Concentration Limit = 6E-13 uCi/ml BHV-2PB
ALARAGoal = 2.25E-14 uCi/ml ALARA Goal-SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARA Goal-1.5E-13 uCi/ml
Pr~ 1994 MPC Urrilt = SE-12 uCi/ml Pre 1994 MPC Limit= BE-14 uCi/ml Pft<~ MPCUmit= 2E-12 uCi/ml pre 1994 MPC Limit= 4E-12 uCi/ml
Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 A LARA GOAL-1E-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
9/30/2008 2.73E-16 9.00E-14 2.25E-14 1.00E-16 2,00E-14 5.00E·15 l.OOE-16 9.00E-13 ,2.25E-13 B.30E-15 6.00E-13 1,50E-13
12/31/2008 5,71E-16 9.00E-14 2.25E-14 1.61E-16 2.00E-14 5.00E-15 1.25E-16 9.00E-13 2.25E-13 2.04E-14 6 OOE-13 1.SOE-13
3/15/2009 3.96E-16 9.00E-14 2.25E-14 1.38E-16 2.00E-14 5.00E-15 1.07E-16 9.00E-13 2,25E-13 4.81E-15 6.00E-13 1.50E-13
6/15/2009 1.24E-17 9.00E-14 2.25E-14 4.64E-17 2.00E-14 S.OOE-15 5.11E-17 9.00E-13 2.25E-13 4.58E-15 o.OOE-13 1.50E·13
9/15/2009 ,2.43E-16 9.00E-14 2.25E-14 5.28E-17 2.00E-14 S.OOE-15 4.84E-17 9.00E-13 2.25E-13 1.19E-14 6.00E-13 1.50E-13
12/15/2009 5.72E-16 9.00E-14 2.25E-14 2.94E-17 2.00E-14 5.00E-15 2.57E-17 9.00E-13 2.25E-13 6.70E-15 6.00E-13 1.50E-13
3/31/2010 S.47E-16 9.00E-14 2.25E-14 1.42E-17 2.00E-14 S.OOE-15 4.66E-17 9.00E-13 2.25E-13 8.24E-15 6.00E-13 1.50E-13
6/30/2010 3.58E-16 9.00E-14 2.25E-14 6.64E-17 2.00E-14 S.OOE-15 9.90E-17 g.OOE-13 2.25E-13 2.01E-15 p.OOE-13 1.50E-13
9/30/2010 2.91E-16 9,00E-14 2.25E-14 4.48E-17 2.00E-14 S.OOE-15 5.72E-17 9.00E-13 2.25E-13 1.08E-15 6.00E-13 1.50E-13
12/3112010 5.73E-16 9.00E-14 2.25E-14 7.24E-17 2.00E-14 S.OOE-15 p,76E-17 9,00E-13 2,25E-13 1.35E-14 6.00E-13 l.SOE-13
4/4/2011 3.79E-16 9.00E-14 2.25E-14 4.01E-17 2.00E-14 5.00E-15 9.11E-17 9.00E-13 2.25E-13 1.06E-14 6.00E-13 l.SOE-13
7/4/2011 3.07E-16 9.00E-14 2.25E-14 8.54E-17 2.00E-14 S.OOE-15 9.21E-17 9.00E-13 2.25E-13 7.21E-15 6.00E-13 1.50E-13
10/3/2011 1.17E-16 9.00E-14 2.25E-14 3.04E-17 2.00E-14 S.OOE-15 2.81E-17 9.00E-13 V5E-13 1.03E-14 6.00E-13 1.50E-13
1/3/2012 3.65E-16 9.00E-14 2.25E-14 2.72E-17 2.00E-14 :S.OOE-15 4.54E-17 9,00E-13 2.25E-13 1.58E-14 6.00E-13 1.50E-13
4/3/2012 4.22E-16 9.00E-14 2.25E-14 1.15E-16 ?-OOE-14 5.00E-15 2.77E-16 9.00E-13 2.25E-13 1.58E-14 6.00E-13 1.50E-13
7/2/2012 3.39E-16 9,00E-14 2.25E-14 1.56E-16 2.00E-14 :S.OOE-15 1.74E-16 9.00E-13 2.25E-13 /3.60E-15 6,00E-13 1.50E-13
10/1/2012 3.13E-16 9.00E-14 2.25E-14 4.13E-17 2.00E-14 S.OOE-15 3.04E-17 9.00E-13 2.25E-13 1.03E-14 6.00E-13 1.50E-13
12/31/2012 2.76E-16 9.00E-14 2.25E-14 5.41E-17 2.00E-14 5.00E-15 7.05E-17 9.00E-13 2.25E-13 1.48E-14 6 OOE-13 1.50E-13
.3/25/2013 3.38E-16 9.00E-14 2.25E-14 3.94E-17 2.00E-14 S.OOE-15 8.32E-17 9.00E-13 2.25E-13 1.42E-14 6.00E-13 1.50E-13
7/2/2013 4.06E-16 9.00E-14 2.25E-14 4.89E-17 2.00E-14 5.00E-15 8.06E-17 9.00E-13 2.25E-13 4.93E-15 6.00E-13 1.50E-13
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TAB3
BHV-3 AIR SAMPLING GRAPHS AND DATA TABLE
Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-3U Effluent Concentration Limit = 2E-14 uCi/ml BHV-3T Effluent Concentration Limit-9E-13 uCi/ml BHV-3R Effluent Concentration Limit-GE-13 uCi/ml BHV-3PB
ALARAGoal = 2.25E-14 uCi/ml ALARA Goal-SE-13 uCi/ml ALARA Goal= 2.25E-13 uCi/ml ALARA Goal-l.SE-13 uCijml
Pi-e 1994 MPC Limit "' SE-12 uCi/ml Pre 1994 MPC Limit= SE-14 uCi/ml P<e-1994 MPC Llinll = 2E-12 uCi/ml Pre a.04 MPC Llml~ 4E-12 uCi/ml
Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 'SE-13 uCi/ml Pre 1994 ALARA GOAL= 1E-12 uCi/ml
Cone EFC EFCA Cone EFC I:FC A Cone EFC EFCA Cone EFC EFCA
9/28/1981 1.74E-15 5.00E-12 1.25E-12 9.02E-16 8.00E-14 ;2.00E-14 2.87E-16 2.00E-12 5.00E-13 1.54E-14 4.00E-12 1.00E-12
12/14/1981 1.59E-15 5.00E-12 1.25E-12 5.03E-16 8,00E-14 .2.00E-14 1.30E-16 2.00E-12 S.OOE-13 2.25E-14 4.00E-12 l.OOE-12 I
3/29/1982 3.76E-16 5.00E-12 1,25E-12 5.25E-16 8.00E-14 .2.00E-14 4.08E-16 2.00E-12 S.OOE-13 1.96E-14 4.00E-12 l.OOE-12
6/30/1982 3.83E-16 5.00E-12 1.25E-12 2.16E-16 8.00E-14 .2.00E-14 1.41E-15 2.00E-12 S.OOE-13 2.40E-14 4.00E-12 l.OOE-12 I
9/27/1982 5.95E-16 5.00E-12 1.25E-12 1.44E-15 8.00E-14 2.00E-14 5.36E-16 2.00E-12 S.OOE-13 1.43E-14 4.00E-12 l.OOE-12
1/3/1983 2.05E-16 5.00E-12 L25E-12 1.23E-16 8.00E-14 2.00E-14 l.lOE-16 2.00E-12 S.OOE-13 3.01E-14 4.00E-12 l.OOE-12 I
4/4/1983 l.OOE-16 5,00E-12 1.25E-12 6.94E-17 8.00E-14 2.00E-14 6.11E-17 2.00E-12 S.OOE-13 L39E-14 4.00E-12 ~.OOE-12
6L30/1983 3.06E-16 5.00E-12 1.25E-12 9.59E-17 8.00E-14 2.00E-14 2.08E-16 2.00E-12 S.OOE-13 1.70E-14 4.00E-12 1.00E-12
10/3/1983 1.91E-16 S.OOE-12 1.25E-12 3.05E-16 8.00E-14 2.00E-14 2.79E-16 2.00E-12 S.OOE-13 1.76E-14 4.00E-12 l.OOE-12
11/3/1984 3.01E-16 5.00E-12 1.25E-12 9.51E-17 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 5 OOE-13 9.17E-15 4.00E-12 1,00E-12
!4/2/1984 8,22E-16 S.OOE-12 1.25E-12 '7.52E-16 8.00E-14 2.00E-14 5.20E-17 2.00E-12 S.OOE-13 3.47E-14 4.00E-12 l.OOE-12
[7/2/1984 5.29E-16 5.00E-12 1.25E-12 p,18E-16 8.00E-14 2.00E-14 1.40E-16 2.00E-12 5.00E-13 1.32E-14 ii.OOE-12 1,00E-12
110/1/1984 1.74E-16 5.00E-12 1.25E-12 7.10E-17 8.00E-14 2.00E-14 l.OOE-16 2,00E-12 5,00E-13 1,08E-14 4.00E-12 l.OOE-12
1/2/1985 l.OOE-17 5.00E-12 "1.25E-12 7.10E-17 8.00E-14 2,00E-14 7.80E-17 2.00E-12 5.00E-13 2.73E-14 ,4.00E-12 l.OOE-12
4/1/1985 l.OOE-16 5.00E-12 1.25E-12 .2.76E-16 8.00E-14 2.00E-14 4.10E-17 2.00E-12 5.00E-13 1.12E-14 4.00E-12 l.OOE-12
7/1/1985 1,04E-16 5.00E-12 1.25E-12 l.OOE-16 B.OOE-14 2.00E-14 l.OOE-16 2.00E-12 5.00E-13 1.64E-14 4,00E-12 l.OOE-12
9/30}1985 l.OOE-16 fi.OOE-12 1.25E-12 l.OOE-15 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 5.00E-13 1.73E-14 4.00E-12 l.OOE-12
1/2/1986 1.03E-15 S.OOE-12 1.25E-12 3.17E-16 8.00E-14 2.00E-14 1.25E-16 2.00E-12 5.00E-13 1.21E-17 ,4,00E-12 l.OOE-12
4/1/1986 8.04E-16 5.00E-12 1.25E-12 L93E-17 8.00E-14 2.00E-14 1.54E-16 2.00E-12 5.00E-13 1.69E-14 4.00E-12 l.OOE-12
6/30/1986 4.29E-16 ~.OOE-12 1.25E-12 1.77E-16 B.OOE-14 2.00E-14 2.83E-16 2.00E-12 5.00E-13 1.97E-14 4.00E-12 l.OOE-12
10/27/1986 6.45E-16 S.OOE-12 1.25E-12 9.89E-17 B,OOE-14 2.00E-14 4,16E-15 2,00E-12 5,00E-13 L64E-14 4.00E-12 l.OOE-12
12/15/1986 L31E-16 S.OOE-12 1.25E-12 O.OOE+OO S.OOE-14 2.00E-14 4.16E-17 2.00E-12 5.00E-13 4.60E-15 4.00E-12 l.OOE-12
3/16}1987 2.01E-16 S.OOE-12 1.25E-12 1.20E-16 8.00E-14 2.00E-14 5.73E-17 2.00E-12 5.00E-13 1.60E-14 4.00E-12 l.OOE-12
5/11/1987 2.16E-16 S.OOE-12 1.25E-12 1.96E-16 S.OOE-14 2,00E-14 7.38E-17 2,00E-12 S.OOE-13 1.59E-14 4.00E-12 l.OOE-12
9/9/1987 2.41E-16 5.00E-12 1.25E-12 2.18E-16 8.00E-14 2.00E-14 3.52E-17 2.00E-12 S,OOE-13 1.46E-14 4,00E-12 1.00E-12
11/2/1987 2ME-16 5.00E-12 1.25E-12 2.32E-16 8.00E-14 2.00E-14 2.37E-17 2.00E-12 5.00E-13 2.48E-14 4,00E-12 1.00E-12
2/16/1988 8.08E-16 S.OOE-12 1.25E-12 2.55E-16 , S.OOE-14 2,00E-14 3.42E-16 2.00E-12 5.00E-13 5.61E-14 4,00E-12 l.OOE-12
5/18/1988 1.14E-16 5.00E-12 1.25E-12 4.14E-17 8.00E-14 2.00E-14 LOOE-16 2.00E-12 5.00E-13 1.20E-14 4.00E-12 1.00E-12
8/15/1988 2.08E-16 S.OOE-12 1.25E-12 3.06E-16 8.00E-14 2.00E-14 S.65E-17 2.00E-12 5.00E-13 L36E-14 4.00E-12 l.OOE-12
11/14/1988 4.21E-16 q.OOE-12 1.25E-12 2.93E-16 8.00E-14 2.00E-14 L09E-16 2.00E-12 5.00E-13 2.48E-14 4.00E-12 l.OOE-12
2/13/1989 4.45E-16 S.OOE-12 1.25E-12 4,78E-17 /l.OOE-14 2.00E-14 2.47E-17 2.00E-12 5.00E-13 3.34E-14 4.00E-12 l.OOE-12
5/15/1989 1.05E-16 5.00E-12 1.25E-12 1.00E-16 8,00E-14 2.00E-14 2.45E-17 2.00E-12 S.OOE-13 6.56E-15 4.00E-12 l.OOE-12
8/14/1989 L31E-16 5.00E-12 1.25E-12 5.85E-17 8.00E-14 2.00E-14 3.97E-17 2.00E-12 S.OOE-13 6.75E-15 4.00E·12 l.OOE-12
11/13/1989 L67E-16 5.00E-12 1.25E-12 3.87E-17 B.OOE-14 2.00E·14 8.03E·17 2.00E-12 5.00E-13 1.69E-14 4.00E·12 l.OOE-12
2/12/1990 4.43E-16 S.OOE-12 1,25E-12 l.OOE-16 8.00E·14 2.00E·14 3.50E-17 2.00E·12 S.OOE-13 ,2,37E-14 4.00E-12 l.OOE-12
5/14/1990 3.84E·16 S.OOE-12 1,25E-12 2.54E-16 B,OOE-14 2.00E-14 L02E-16 ~.OOE-12 S.OOE-13 1,68E·14 4.00E-12 1,00E-12
8/13/1990 7.27E·17 S.OOE-12 1,25E·12 2.87E-16 8.00E-14 2.00E-14 L21E-17 2.00E-12 S.OOE-13 7.86E·15 4.00E-12 LOOE-12
11/12/1990 L84E-16 S.OOE-12 1.25E-12 L34E-16 8.00E-14 2.00E-14 8.53E-17 i!.DOE-12 S.OOE-13 ,2.01E-14 4.00E-12 l.OOE-12
2/11/1991 4.66E-17 5.00E-12 1.25E·12 8.48E-16 8.00E-14 2.00E-14 1.94E-17 2.00E·12 5.00E-13 3.69E-14 4.00E-12 l.OOE-12
5/13/1991 ~.05E-17 5.00E-12 1.25E-12 7.40E·17 8.00E·14 2.00E·14 7.00E·18 2.00E-12 S,OOE-13 l.SOE-14 4.00E·12 1 OOE-12
8/12/1991 7.14E-17 5,00E-12 1.25E-12 6.22E-17 8.00E-14 2.00E-14 7.95E-17 2.00E-12 S.OOE-13 L77E-14 4.00E-12 1.00E-12
11/11/1991 1.41E-17 S.OOE-12 1.25E-12 2,19E-18 8.00E-14 2,00E-14 2.75E-17 2.00E-12 S.OOE-13 1.18E-14 4.00E-12 l.OOE-12
2/10/1992 8.12E-17 5.00E-12 1.25E-12 2,35E-17 8.00E-14 2.00E-14 2.76E-18 2.00E-12 5.00E-13 3.57E-14 4.00E-12 1.00E-12
5/11/1992 9.18E-17 5,00E-12 1.25E-12 5,80E-17 8.00E-14 2.00E-14 3.36E-17 2.00E-12 5.00E-13 1.28E-14 4.00E-12 l.OOE-12
8/10/1992 2.00E-18 5.00E-12 1.25E-12 4.19E-17 8,00E-14 2.00E-14 2.00E-18 2.00E-12 5.00E-13 1.59E-14 4.00E-12 l.OOE-12
11/9/1992 4.00E-17 5.00E-12 1.25E-12 2.68E-17 8,00E-14 2.00E-14 1.07E-17 .2.00E-12 5,00E-13 L81E-14 4.00E-12 l.OOE-12
2/9/1993 7.94E-17 5.00E-12 1,25E-12 l.OOE-16 8.00E-14 f.OOE-14 1.09E-16 ;I..OOE-12 :S.OOE-13 2.69E-14 4.00E-12 l.OOE-12
5/10/1993 1.60E-17 5.00E-12 1.25E-12 5.07E-17 8.00E-14 2.00E-14 7.64E-17 2.00E-12 5.00E-13 1.26E-14 4.00E-12 l.OOE-12
S/10/1993 6.00E-17 5.00E-12 1.25E-12 6.00E-18 8.00E-14 2.00E-14 l.OOE-16 2.00E-12 .S.OOE-13 1.50E-14 4.00E-12 l.OOE-12
11/8/1993 l.OOE-16 5.00E-12 1.25E-12 l.OOE-16 8.00E-14 .2 OOE-14 l.OOE-16 2.00E-12 5.00E-13 2.10E-14 4.00E-12 l.OOE-12
2/7/1994 1.61E-16 5.00E-12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 2.22E-16 2.00E-12 S.OOE-13 2.23E-14 4.00E-12 ,l.OOE-12
s/9/1994 2.77E-16 5.00E-12 1.25E-12 2.80E-17 8.00E-14 2.00E-14 8.37E-18 2 OOE-12 5.00E-13 1.40E-14 4.00E-12 1.00E-12
8/9/1994 739E-17 5.00E-12 1.25E-12 l.OOE-16 S,OOE-14 2.00E-14 1.14E-16 2.00E-12 5.00E-13 1.00E-16 4.00E-12 LOOE-12
11/7/1994 9.05E-17 5.00E-12 1.25E-12 l.OOE-16 l'!.OOE-14 2.00E-14 l.OOE-16 2.00E-12 5.00E-13 l.OOE-16 4,00E-12 l.OOE-12
Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-3U Effluent Concentration Limit = ZE-14 uCi/ml I!HV-3T Effluent Concentration Limit= 9E-13 uCi/ml BHV-3R Effluent Concentration Limit = 6E-13 uCi/ml BHV-3PB
ALARAGoal = ll.ZSE-14 uCi/ml ALARA Goal= SE-13 uCi/ml ALARAGoal = Z.ZSE-13 uCi/ml /'.LARA Goal= l.SE-13 uCi/ml
Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC Limit -BE-14 uCi/ml ·Pre 1994 MPC Limit= ZE-12 uCi/ ml Pre 1994 MPC Limit= 4E-12 uCi/ml
_pre 1994 A LARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
2/7/1995 7.99E-17 9.00E-14 2.25E·14 9.60E-17 2.00E-14 S.OOE-15 9.60E-17 9,00£.-U 2.25E-13 9.05E-15 6.00E-13 1.50E-13
5/9/1995 9.40E-17 9 OOE-14 2.25E-14 9.80E-17 2.00E-14 S.OOE-15 8.60E-17 !J.OOE-13 2.25E-13 2.88E-15 6.00E-13 1.50E-13
8/9/1995 7.30E·17 9.00E-14 2.25E-14 ~.20E-17 2.00E·14 S.OOE-15 4.40E-17 9.00E-13 2.25E-13 1.96E-15 G.OOE-13 l.SOE-13
)1/11/1995 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E·14 S.OOE-15 6.58E-17 9.00E-13 2 25E-13 1.91E-14 G.OOE-13 1.50E-13
,2/5/1996 3.41E-16 9.00E-14 2.25E-14 2.26E-16 Z.OOE-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 G.OOE-13 1.50E-13
S/6}l'J96 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1,82E-16 9.00E-13 2.25E-13 1,53E-14 G.OOE-13 1.50E-13
8/5/1996 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 G.OOE-13 1.50E-13
U/6/1996 3.16E-16 9.00E-14 2.25E-14 1.31E-16 .2.00E-14 5.00E-15 6.58E-17 9 OOE-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13
2/6/1997 3.41E-16 9.00E-14 .2.25E-14 2.26E-16 2.00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13
5/5/1997 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6,00E-13 1 50E-13 1
8/11/1997 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13
1/5/1998 3.16E-16 9.00E-14 2.25E·14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 S.OOE-13 2.25E-13 1.91E-14 6.00E-13 1.50E·13
4/28/1998 .3.41E-16 9.00E-14 2.25E·14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13
7/31/1998 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2,25E-13 1.53E-14 6.00E-13 1.50E-13
9/28/1998 3.00E·16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 p,OOE-13 1.50E·13
12/28/1998 3.16E·16 9.00E-14 2.25E·14 1.31E-16 2.00E-14 S.OOE-15 .6.58E-17 9.00E-13 2.25E-13 1.91E-14 G.OOE-13 1.50E·13
3/29/1999 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E·13
7/3/1999 1.31E-16 9.00E·14 2.25E·14 1.39E·16 2.00E·14 S.OOE-15 1.82E·16 9.00E-13 2.25E-13 1.53E·14 G.OOE-13 1.50E-13
9/27/1999 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13
12/28/1999 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 S.OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6 OOE-13 1.50E-13
3/28/2000 3.41E-16 9,00E-14 2.25E·14 2.26E-16 2.00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6 OOE-13 1.50E-13
6/26/2000 1.31E-16 9.00E-14 2.25E·14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13
fJ/26/2000 3.00E·16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9,00E-13 2.25E-13 1,31E-14 6.00E-13 1.50E-13
12/26/2000 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9.00E-l3 2.25E-13 1.91E-14 6.00E-13 l.SOE-13
3/26/2001 3.41E-16 9.00E-14 2.25E-14 2.26E-16 ~.OOE·14 5,00E-15 1.18E-16 9.00E-l3 2.25E-l3 2.69E-14 6.00E-13 1.50E-13
7/2/'1.001. 1.31E-16 9.00E-14 2.25E·14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-l3 1.53E·14 6,00E-l3 1.50E-13
9/24/2001 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5,00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-l3 1.50E-13
12/31/2001 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E·14 5.00E-15 6,58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13
4/1/2002 3.41E-16 iJ.OOE-14 2.25E-14 2.26E-16 2.00E·14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 2,69E-14 6.00E-13 1.50E-13
7/1/2002 1.31E-16 S.OOE-14 2.25E-14 1.39E-16 2.00E·14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 153E-14 6.00E-13 1.50E-13
9/30/2002 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E·14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 L31E-14 6.00E-13 1.50E-13
12/30/2002 3.16E-16 \l.OOE-14 2.25E-14 1.31E-16 2.00E-14 5,00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1,50E-13
3/31/2003 3.41E-16 IJ,OOE-14 2.25E-14 2.26E-16 2.00E-14 5,00E-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13
6/30/2003 1.31E-16 9,00E-14 2.25E·14 1,39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E·14 6.00E-13 1.50E·13
9/29/2003 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9,00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13
12/29/2003 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E·14 5.00E-15 6.58E·17 !WOE-13 2.25E-13 l.91E-14 6.00E·13 1,50E-13
3/29/2004 3.41E·16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-l3 2.69E-14 6.00E-13 1.50E-13
6/27/2004 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 l.82E-16 9.00E-l3 l.25E-13 1.53E-14 6.00E-13 1.50E-13
9/27/2004 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 ~.OOE-15 3.99E-16 ~.OOE-13 2,25E-13 1.31E-14 6.00E-13 1.50E-13
12/27/2004 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 ii.OOE-15 6,58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13
3/28/2005 .3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 1.18E-16 '3.00E-13 2.25E-13 2.69E-14 p.OOE-13 1.50E-13
6/29/2005 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 !i.OOE-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13
9/26/2005 3.00E-16 9.00E-14 2,25E-14 3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9.00E-13 2 25E-13 1.31E-14 6.00E-13 1.50E·13
1/3/2006 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 6.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 t.SOE-13
4/3/2006 3.41E-16 9.00E-14 2.25E·14 2.26E-16 2.00E-14 S.OOE-15 1.18E-16 9.00E-13 2.25E-13 2.69E-14 6.00E-13 1.50E-13
7/3/2006 1.31E-16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-13 2.25E-13 1,53E-14 6.00E-13 l.SOE-13
10/2/2006 3.00E·16 9.00E-14 2.25E-14 .3.43E-16 2.00E-14 S.OOE-15 3.99E-16 9,00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13
1/1/2006 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2.00E-14 S.OOE-15 6.58E-17 9 OOE-13 2,25E-13 1.91E-14 6.00E-l3 1.50E-13
4/2/2007 3.41E-16 9.00E-14 2.25E-14 2.26E·16 2.00E·14 S.OOE-15 1.18E-16 9.00E·13 2.25E-13 2.69E-14 6.00E-13 1.50E-13
7/2/2007 1.31E-16 9.00E-14 2.25E·14 139E-16 2.00E-14 S.OOE-15 1.82E-16 9.00E-l3 2.25E-13 1.53E-14 6.00E-13 1.SOE-13
9/30/2007 3.00E-16 9.00E·14 2.25E-14 3.43E-16 2.00E-14 5.00E-15 3.99E-16 9.00E-13 2,25E-l3 1,31E-14 6.00E-13 1.50E-13
12/31/2007 3.16E-16 I'~.OOE-14 2.25E-14 1.31E·16 2.00E·l4 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.SOE-13
3/31/2008 3.41E-16 I9.00E-14 2.25E-14 2.26E-16 2.00E-14 S,OOE-15 1.18E-16 9.00E-13 2.25E-l3 2.69E-14 6,00E-13 1.50E-13
6/30/2008 1.31E-16 _ _ j9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 -
Date Effluent Concentration limit-9E-14 uCi/ml BHV-3U Effluent Concentration Limit= 2E-14 uCi/ml ~HV-3T Effluent Concentration Limit = 9E-13 uCi/ml BHV-3R Effluent Concentration limit-6E-13 uCi/ml ~HV-3PB I
ALARAGoal = 2.25E-14 uCi/ml ALARA Goal= SE-13 uCi/ml ALARAGoal-2.25E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml
I
Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC limit= BE-14 uCi/ml Pre 1994 MPC limit= ZE-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml
Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL= 1E-12 uCi/ml
Cone EFC EFCA Cone ~FC EFCA Cone EFC EFCA Cone EFC EFCA !
9/30/2008 3.00E-16 9.00E-14 2.25E-14 3.43E-16 .2.00E·14 5,00E-15 3.99E-16 9.00E-13 2,25E-13 1.31E-14 6.00E-13 1.50E-13 i
12/31/2008 3.16E-16 9.00E-14 .2.25E-14 1.31E-16 .2.00E-14 s.OOE-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 I
3/15/2009 3.41E-16 9.00E-14 .2.25E-14 2.26E-16 2.00E-14 5.00E-15 l.lBE-16 9.00E-13 2.25E-13 2.69E-14 6,00E-13 1.50E-13 I
6/.15/,UIW 1.31E-16 9.00E-14 .2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.50E-13 :
9/15/2009 3.00E-16 S.OOE-14 2.25E-14 3,43E-16 2.00E-14 5.00E-15 3,99E-16 9,00E-13 2.25E-13 1.31E-14 6.00E-13 1.50E-13
12/15/2009 3.16E-16 9.00E-14 2.25E-14 1.31E-16 2,00E-14 5.00E-15 6.58E-17 9.00E-13 2.25E-13 1.91E-14 6.00E-13 1.50E-13 ,
3/31/2010 3.41E-16 9.00E-14 2.25E-14 2.26E-16 Z.OOE-14 5,00E-15 l.lBE-16 9.00E-13 2.25E-13 2.69E-14 6,00E-13 1.50E·13 I
6/30/2010 1.31E·16 9.00E-14 2.25E-14 1.39E-16 2.00E-14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E-14 6,00E-13 1.50E·13
.9/30/2010 3.00E-16 9.00E-14 2.25E-14 3.43E-16 2.00E·14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1,31E-14 6.00E-13 1.50E·13
12/31/2010 3.16E·16 9.00E-14 2.25E·14 1.31E-16 2.00E-14 5.00E-15 6.58E-17 9,00E-13 2.25E·l3 1.91E·14 6.00E-13 1.50E-13
4/4/2011 3.41E-16 9.00E-14 2.2SE·14 2.26E-16 2.00E·14 5.00E-15 l.lBE-16 9.00E-13 :Z.25E-13 2.69E-14 6.00E·l3 l.SOE-13
7/4/2011 1.31E·16 9,00E-14 2.25E·14 1.39E-16 2.00E·14 5.00E-15 1,82E-16 9.00E·13 .2.25E-13 1.53E·14 6.00E-13 1.50E-13
10/3/2011 3.00E-16 9.00E-14 2.25E·14 3.43E-16 2.00E·14 5.00E-15 3.99E-16 9.00E-13 2.25E-13 1.31E-14 6.00E-13 l.SOE·13
1/3/2012 3.16E·16 9.00E·14 2.25E·14 1.31E-16 2,00E·14 S.OOE-15 6.58E·17 9.00E-13 2.25E-13 L91E·14 6.00E-13 1.50E-13
4/3/2012 3.41E-16 9.00E-14 2.25E-14 2.26E-16 2.00E-14 5.00E-15 l.lSE-16 9.00E-13 2.25E-13 2,69E-14 G.OOE-13 1.50E·13
7/2/2012 1.31E-16 9.00E-14 2.25E·14 1.39E-16 2.00E·14 5.00E-15 1.82E-16 9.00E-13 2.25E-13 1.53E·14 5.00E-13 1.50E-13
10/1/2012 3,00E-16 9,00E-14 2.25E-14 3.43E-16 2.00E·14 5.00E-15 3,99E-16 9.00E-13 2.25E-13 1.31E·14 6.00E-13 1.50E-13
12/31/2012 3.16E·16 9.00E·14 2.25E·14 1.31E-16 .2.00E·14 5.00E-15 6.58E-17 9,00E-13 2.25E·13 1.91E·14 G.OOE-13 1.50E-13
3/25/2013 3.41E·16 9.00E·14 2.25E·14 2.26E-16 2.00E·14 5.00E-15 1.18E-16 9.00E-13 2.25E·13 2.69E-14 6.00E-13 1.50E-13
7/2/2013 1.31E·16 9.00E-14 2.25E-14 1.39E-16 2.00E·14 5.00E-15 1.82E-16 9.00E-13 2,25E-13 1.53E-14 6,00E-13 1.50E·13
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TAB4
BHV-4 AIR SAMPLING GRAPHS AND DATA TABLE
Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-4U Effluent Concentration Limit= 2E-14 uCijml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit= 6E-13 uCi/ml BHV-4PB
ALARAGoal = 2.25E-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal-Z.ZSE-13 uCi/ml ALARA Goal-l.SE-13 uCi/ml
Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC Limit-SE-14 uCi/ml Pre 1994 MPC Limit= ZE-12 uCi/ml ·Pre 1994 MPC Limit= 4E-12 uCi/ml
Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL= 1E-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC 'EFCA
9}28/1981 5.20E-15 S.OOE-12 1.25E-12 2.93E-15 B.OOE-14 2.00E-14 2.74E-15 2.00E-12 S.OOE-13 1.84E-14 4.00E-12 l.OOE-12
12/14/.1981 4.53E-15 S.OOE-12 L2SE-12 1.78E-15 8.00E-14 2.00E-14 2.29E-15 2.00E·12 S.OOE-13 2.54E-14 fi,OOE-12 l.OOE-12
?1/29/1987. 1,06E-15 S.OOE-12 1.25E-12 1.42E-14 8.00E-14 2.00E-14 1,07E-15 2.00E-12 S.OOE-13 2.31E-14 4.00E-12 l.OOE-12
6/3lJ/19S'l 6.03E-15 5.00E-12 1.25E-12 1.57E-14 B.OOE-14 2.00E-14 2.62E-15 2.00E-12 S.OOE-13 2.25E-14 4.00E-12 1 OOE-12
9/27/1982 1.26E-14 S.OOE-12 1.25E-12 7.58E-16 8.00E-14 2.00E-14 5.35E-15 2-00E-12 S.OOE-13 2.68E-14 4.00E-12 1.00E-12
1/3/1983 4.33E-15 S.OOE-12 1.25E-12 6.52E-16 8.00E-14 2.00E-14 6.04E-16 2.00E-12 S.OOE-13 2.57E-14 4.00E-12 1.00E-12
4/4/1983 1,25E-15 S.OOE-12 1.25E-12 7,17E-16 B.OOE-14 2.00E-14 6.76E-16 2.00E-12 S.OOE-13 2.00E-14 4.00E-12 l.OOE-12
6/3011983 3.73E-16 S.OOE-12 1.2SE-12 9.43E-16 8.00E-14 2.00E-14 4.13E-16 2.00E-12 S.OOE-13 1.20E-14 4.00E-12 1.00E-12
10/3/1983 2.54E-16 S.OOE-12 1,25E-12 1.51E-16 8.00E-14 2.00E-14 2.65E-16 2.00E-12 S.OOE-13 l.SOE-14 4.00E-12 1.00E-12
1/3/1984 .2.76E-15 S,OOE-12 1.25E-12 1.60E-16 8.00E-14 2.00E-14 l.OSE-16 2.00E-12 S.OOE-13 1.59E-16 4.00E-12 l.OOE-12
4/2/1984 4.27E-16 S.OOE-12 1.25E-12 2.33E-16 8.00E-14 2.00E-14 6,28E-16 2.00E-12 5.00E-13 3.67E-14 4.00E-12 l.OOE-12
7}2/1984 2.57E-15 5.00E-12 1.25E-12 1.36E-16 8,00E-14 2.00E-14 1.11E-16 2.00E-12 'S.OOE-13 1.58E-14 4.00E-12 l.OOE-12
10/1/1984 4.18E-16 5.00E-12 1.25E-12 3.54E-16 8.00E-14 2.00E-14 l.lOE-17 2.00E-12 5.00E-13 9.83E-15 4.00E-12 l.OOE-12
l/2/19HS 5.30E-17 5.00E-12 1.25E-12 3.55E-17 8.00E-14 2.00E-14 7.00E-18 2.00E-12 5.00E-13 2.57E-14 4.00E-12 l.OOE-12
4/1/1985 1,00E-16 S.OOE-12 1.25E-12 6.00E-16 8.00E-14 2.00E-14 ,4.35E-17 2 OOE-12 5,00E-13 5.02E-15 4.00E-12 l.OOE-12
7/1/1985 9.36E-16 5.00E-12 1.25E-12 2.33E-16 B.OOE-14 2.00E-14 2.36E-16 2.00E-12 S.OOE-13 7.48E-15 4.00E-12 1,00E-12
9/30/1985 1.46E-15 S.OOE-12 1.25E-12 7.69E-16 ll.OOE-14 Z.OOE-14 5.38E-16 2.00E-12 5,00E-13 7,86E-15 4.00E-12 l.OOE-12
1/2/1986 8.40E-15 S.OOE-12 1.25E-12 7.60E-16 B.OOE-14 2.00E-14 2.99E-16 2.00E-12 5.00E-13 2.12E-14 4,00E-12 1.00E-12
4/1/1986 5.79E-15 S.OOE-12 1.25E-12 5.80E-16 S.OOE-14 2.00E-14 1.34E-15 2.00E·12 5.00E-13 1.33E-14 4.00E-12 l.OOE-12
6/3D/l.!i85 5.19E-15 S.OOE-12 1.25E-12 7.83E-16 S.OOE-14 2.00E-14 2.20E-15 2.00E-12 5.00E-13 7,14E-16 4.00E-12 l.OOE-12
10/27/1986 4.60E-15 S.OOE-12 1.25E-12 4.67E-16 8.00E-14 2.00E-14 2.37E-15 2.00E-12 S.OOE-13 1,13E-14 4.00E-12 1.00E-12
12/15/1986 2.75E-15 5.00E-12 1.25E-12 5.90E-16 S.OOE-14 2.00E-14 9.39E-16 2.00E-12 5.00E-13 1.20E-14 4.00E-12 l.OOE-12
3/16/1987 4.64E-15 5.00E-12 1.25E-12 1.18E-15 B,OOE-14 2.00E-14 4.97E-16 2.00E-12 5.00E-13 5.89E-14 4.00E-12 l.OOE-12
5/11/1987 4.35E-15 5.00E-12 1.25E-12 1.23E-14 8.00E-14 2.00E-14 1.13E-15 2.00E-12 S.OOE-13 2.21E-14 4.00E-12 l.OOE-12
9/9/1987 6.39E-15 5.00E-12 1.25E-12 1.50E-14 B.OOE-14 Z.OOE-14 _2.26E-15 l.OOE-12 .5.00E-13 1.57E-14 4.00E-12 l.OOE-12
11/2/1987 6.72E-15 5.00E-12 1.25E-12 4.53E-16 8.00E-14 2.00E-14 2.20E-15 2.00E-12 5.00E-13 2.55E-14 4.00E-12 1.00E-12
2/16/1988 1.91E-15 5.00E-12 1.25E-12 1.35E-14 8.00E-14 2.00E-14 4.42E-16 Z.OOE-12 S.OOE-13 4.44E-14 4.00E-12 l.OOE-12
5/18/1988 1.78E-14 5.00E-12 1.25E-12 4.39E-14 8.00E-14 2.00E-14 4.92E-16 2.00E-12 S.OOE-13 1,38E-14 4.00E-12 LOOE-12
8/15/1988 7.56E-15 5.00E-12 1.25E-12 3.31E-14 8.00E-14 2.00E-14 1.51E-15 2.00E-12 5.00E-13 1.97E-14 4.00E-12 l.OOE-12
11/14/1988 1.47E-14 5.00E-12 1.25E-12 1.56E-15 8.00E-14 2.00E-14 2,57E-15 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 l.OOE-12
2/13/1989 2.47E-15 5.00E-12 1.25E-12 3.14E-15 8.00E-14 2.00E-14 6.94E-16 Z.OOE-12 5.00E-13 2.12E-14 4,00E-12 l.OOE-12
5/15/1989 2.50E-16 5.00E-12 1.2SE-12 7.68E-15 8.00E-14 2.00E-14 9.03E-16 2.00E-12 S.OOE-13 8.05E-15 4.00E-12 1.00E-12
8/14/1989 6.50E-15 S.OOE-12 l.l5E-12 4.72E-15 B.OOE-14 2.00E-14 2.35E-15 2.00E-12 5.00E-13 9,95E-15 4.00E-12 l.OOE-12
11/13/1989 9.63E-15 5.00E-12 1.25E-12 4.05E-15 8.00E-14 2.00E-14 4.03E-15 2.00E-12 5.00E-13 1.99E-14 4.00E-12 1.00E-12
2/12/1990 8.92E-15 5.00E-12 1.25E-12 3.56E-15 8.00E-14 2.00E-14 2,89E-15 2.00E-12 S.OOE-13 2.69E-14 4 OOE-12 l.OOE-12
5/14/1990 8.90E-15 S.OOE-12 1.25E-12 3.58E-15 8.00E-14 2.00E-14 2.33E-15 2.00E-12 5.00E-13 2.09E-14 4.00E-12 l.OOE-12
~/1.990 1.92E-15 5,00E-12 1.25E-12 1.87E-15 8.00E-14 2.00E-14 5.06E-16 Z.OOE-12 5,00E-13 8.86E-15 4.00E-12 1.00E-12
l!ll11!!99o 2,91E-15 S.OOE-12 1.25E-12 2.25E-17 B.OOE-14 2.00E-14 l.OBE-15 2.00E-12 S.OOE-13 2.19E-14 4.00E-12 l.OOE-12
2/11/1991 1.67E-16 5.00E-12 1.25E-12 7,89E-16 8.00E-14 2.00E-14 p.38E-17 2.00E-12 5.00E-13 4.19E-14 4.00E-12 l.OOE-12
5/13/1991 1.87E-16 5.00E-12 1,25E-12 2.61E-15 8.00E-14 2.00E-14 3.54E-16 2.00E-12 5.00E-13 1.40E-14 4.00E-12 1,00E-12
8/12/1991 4.85E-16 5.00E-12 1.25E-12 4.38E-16 8.00E-14 2.00E-14 1.27E-16 2.00E-12 5.00E-13 2.20E-14 4.00E-12 1.00E-12
11/11/1991 1.77E-16 5.00E-12 1.25E-12 1.46E-16 8.00E-14 2.00E-14 3.76E-17 2.00E-12 S.OOE-13 1.15E-14 4,00E-12 l.OOE-12
2/10/1992 1.83E-16 5.00E-12 1.25E-12 1.95E-15 B.OOE-14 2.00E-14 1.33E-16 Z.OOE-12 S.OOE-13 3.35E-14 4.00E-12 1.00E-12
5/11/1992 4.40E-16 5.00E-12 1.25E-12 2.56E-16 B.OOE-14 2.00E-14 4.04E-16 2.00E-12 5.00E-13 1.41E-14 4.00E-12 l.OOE-12
8/10/1992 9.09E-17 S,OOE-12 1.25E-12 1.15E-16 8.00E-14 2.00E-14 4.50E-17 2.00E-12 5.00E-13 1.57E-14 4.00E-12 l.OOE-12
11/9/1992 2.07E-16 5.00E·12 1.25E-12 l.OOE-16 8.00E-14 2.00E-14 3,62E-17 2.00E-12 5.00E-13 2.24E-14 4.00E-12 l.OOE-12
2/9/1993 1.73E-16 5.00E-12 1.25E-12 2.76E-17 B.OOE-14 2.00E-14 2.89E-17 2.00E-12 5.00E-13 3.08E-14 4 OOE-12 l.OOE-12
5/J0/1.993 2.70E-17 5.00E-12 1.25E-12 2.50E-17 B.OOE-14 2.DOE-14 8.74E-17 2.00E-12 5.00E-13 1.25E-14 4.00E-12 1.00E-12
B/10/1993 9.00E-17 5.00E-12 1.25E-12 l.76E-16 B.OOE-14 2 OOE-14 O.OOE+OO 2.00E-12 5.00E-13 1.50E-14 4.00E-12 l.OOE-12
11/8/1993 1,00E-16 'S.OOE-12 1.25E-12 l.OOE-16 B.OOE-14 2.00E-14 6.00E-17 2,00E-12 5.00E-13 1.75E-14 4.00E-12 l.OOE-12
2!1/JIJ91< 1.10E-16 S.OOE-12 1.25E-12 3.38E-16 B.OOE-14 2.00E-14 2.21E-16 2.00E-12 5.00E-13 3.08E-14 4,00E-12 l.OOE-12
!i/9/1994 3.80E-16 5.00E-12 1.25E-12 2.82E-16 B.OOE-14 2,00E-14 3.46E-16 2.00E-12 5.00E-13 1.73E-14 4 OOE-12 l.OOE-12
8/9/1994 3.85E-16 5.00E·12 1.25E-12 3.53E-16 S,OOE-14 2.00E-14 l.OOE-16 2.00E-12 5.00E-13 1.00E-16 4.00E-12 1,00E-12
11/7/1994 6,21E-17 5.00E-12 1.25E-12 9.70E-17 8,00E-14 2.00E-14 1.96E-16 .2.00E-12 _ S.OOE-13 l.OOE-16 --4.00E-12 l.OOE-12
Date Effluent Concentration limit= 9E-14 uCi/ml BHV-4U Effluent Concentration limit -ZE-14 uCi/ml BHV-4T Effluent Concentration Limit = !IE-13 uCi/ml BHV-4R Effluent Concentration Limit-6E-13 uCi/ml BHV-4PB I
ALARAGoal = 2.25E-14 uCi/ml ALARA Goal-SE-13 uCi/ml ALARAGoal = :Z.25E-13 uCi/ml ALARA Goal-l.SE-13 uCi/ml
I Pre 1994 MPC limit= SE-12 uCi/ml Prel994 MP.C Umlt£ SE-14 uCi/ml Pre 1994 MPC Limit = ~E-12 uCi/ml Pre 1994 MPC Llmit = 4E-12 uCi/ml
Pre 1994 A LARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL= lE-12 uCi/ml I
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
2/7/1995 3.70E-16 9,00E-14 2.25E-14 9.80E-17 2.00E-14 5.00E-15 9.70E-17 9.00E-.13 2.25E-13 8.84E-15 6.00E-13 1.50E-13
5/9/1995 9.40E-17 9.00E-14 2.25E-14 2.86E-16 2.00E-14 5.00E-15 1.90E-16 9.00E-13 2.25E-13 2.90E-15 p.OOE-13 1.50E-13
IB/9/1995 1.45E-16 9.00E-14 2.25E-14 .2.31E-15 2.00E-14 5.00E-15 7.10E-17 9.00E-13 2.25E-13 2.70E-15 6.00E-13 L50E-13
11/11/1995 1.43E-14 9.00E-14 2.25E-14 5.70E-15 2.00E-14 5.00E-15 2.61E-15 9.00E-13 2.25E-13 5 60E-15 6.00E-13 1.50E-13
2/5/1996 1.19E-14 9.00E-14 2.25E-14 3.80E-16 2.00E-14 5.00E-15 6.10E-15 9.00E·13 2.25E-13 6.48E-15 6.00E-13 1.50E-13
51,6/1!*6 4.55E-16 9.00E-14 2.25E-14 3.57c-15 2.00E-14 5.00E-15 2.84E-16 9,00E-13 2,25E-13 7,68E-15 6.00E-13 150E-13
8/5/1996 7,78E-16 g.OOE-14 2.25E-14 3.51E-15 2.00E-14 5.00E-15 1.69E-16 9.00E-13 2.25E-13 4.90E-15 6.00E-13 1.50E-13
11/6/1996 1.36E-15 9.00E-14 225E-14 l.OOE-16 2.00E-14 5.00E-15 4.21E-16 9.00E-13 2.25E-13 1.10E-14 6 OOE-13 1.50E-13
2/6/1997 l.OOE-16 9.00E-14 2.25E-14 1.40E-16 2.00E-14 5.00E-15 1.03E-16 9.00E-13 2.25E-13 6.76E-15 6.00E-13 1.50E-13
5/5/1997 l.OOE-16 9.00E·l4 2.25E-14 4.00E-16 2.00E-14 5.00E-15 .2.24E-16 9,00E-13 2.25E-13 4.55E-15 6.00E-13 1,50E-13
8/11/1997 4.74E-16 9.00E-14 2.25E-14 9.07E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.55E-15 6.00E-13 1.50E-13
1/5/1998 8.31E-16 9.00E-14 2.25E-14 4.82E-16 2.00E-14 S.OOE-15 1.77E-16 9.00E-13 2.25E-13 S.28E-15 6.00E-13 1.50E-13
4/28/1998 3.32E-16 9.00E-14 2.25E-14 4.43E-15 2.00E-14 5.00E-15 1.21E-16 9.00E-13 2.25E-13 7.43E-15 6.00E-13 1.50E-13
7/31/1998 4.60E-16 9.00E-14 2.25E-14 9.02E-16 2.00E-14 S.OOE-15 3.54E-16 9.00E-13 .2.25E-13 6.91E-15 6.00E-13 1.SOE-13
9/28/1998 4.08E-16 9.00E-14 2.25E-14 4.93E-16 Z.OOE-14 &.OOE-15 2.53E-16 9.00E-13 ,2.25E-13 4.52E-15 6.00E-13 1.50E-13
12/28/1998 7.72E-16 9,00E-14 2.25E-14 3.75E-16 2.00E-14 5.00E-15 3.43E-16 9.00E-13 2.25E-13 6.73E-15 6.00E-13 1.50E-13
3/29}1999 5.11E-16 9.00E-14 2.25E-14 4.70E-16 2.00E-14 5.00E-15 3.70E-16 9.00E-13 2.25E-13 8.96E-15 6.00E-13 1.50E-13
7)3/1999 5.90E-16 9.00E-14 2.25E-14 9.89E-16 .2.00E-14 S.OOE-15 1.28E-16 9.00E-13 2.25E-13 6.40E-15 6.00E-13 1.50E-13
9/27/1999 1.70E-15 9.00E-14 2.25E-14 7.50E-16 2.00E-14 5.00E-15 4.61E-16 9,00E-13 2.25E-13 7 86E-15 6.00E-13 1.50E-13
l7./28/19S"J 1.03E-15 9.00E-14 2.25E-14 7.50E-16 l.OOE-14 5,00E-15 2.43E-16 9.00E-13 2.25E-13 6.42E-15 6.00E-13 l.SOE-13 -
3/27/2000 1.00E-16 9.00E-14 2.25E-14 2.13E-16 2.00E-14 5.00E-15 2.20E-16 9.00E-13 2.25E-13 5,61E-15 6.00E-13 1.50E-13
6/26/2000 1.75E-16 9.00E-14 2.25E-14 3.08E-16 2.00E-14 S.OOE-15 1.11E-16 9.00E-13 2.25E-13 3.92E-15 6.00E-13 1,50E-13
9/26/2000 3.65E-16 9.00E-14 2.25E-14 2.01E-16 2.00E-14 5,00E-15 2.24E-16 9 OOE-13 2.25E-13 7.79E-15 6,00E-13 1.50E-13
12/26f.20lxJ 2,27E-16 9.00E-14 2.25E-14 1,00E-16 2.00E-14 5.00E-15 4.35E-16 9.00E-13 2.25E-13 8.45E-15 6,00E-13 1.50E-13
3/26/2001 1.45E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 l.OOE-16 9,00E-13 2.25E-13 6.37E-15 6.00E-13 1.50E-13
7/2/2001 l.OOE-16 9.00E-14 2,25E-14 1.05E-16 2.00E-14 5.00E-15 l.OOE-16 9 OOE-13 .2.25E-13 6.99E-15 6.00E-13 1.50E-13
9/24/2001 1.91E-16 9,00E-14 2,25E-14 l.OOE-16 2.00E-14 S.OOE-15 2.01E-16 9.00E-13 2.25E-13 8.04E-15 6.00E-13 1.50E-13
12/31/2001 1.38E-16 9.00E-14 2.25E-14 2.05E-16 2.00E-14 S.OOE-15 l.OOE-16 ~.OOE-13 2.25E-13 1.83E-15 6.00E-13 1.50E-13
4/1/2002 2.20E-16 9,00E-14 2.25E-14 3.38E-16 2.00E-14 S.OOE-15 L26E-16 9.00E-13 2.25E-13 7.48E-15 6.00E-13 1.50E-13
7/1/2002 1.97E-16 9.00E-14 2.25E-14 4.10E-16 2,00E-14 S.OOE-15 l.OOE-16 9.00E-13 2,25E-13 7.40E-15 6.00E-13 1.50E-13
9/30/2002 2.30E-16 9.00E-14 2,25E-14 2.42E-16 2.00E-14 5.00E-15 1.56E-16 9.00E-13 2.25E-13 4.21E-15 6.00E-13 1.50E-13
~30/2002 l.OOE-16 9.00E-14 2.25E-14 1.92E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 9.42E-15 6.00E-13 1.50E-13
3/31/2003 2.50E-16 9 OOE-14 2.25E-14 1.69E-16 2.00E-14 S.OOE-15 1.29E-16 9.00E-13 2.25E-13 4.55E-15 6.00E-13 l.SOE-13
6/30/2003 l.OOE-16 9.00E-14 2.25E-14 2.87E-16 2.00E-14 S.OOE-15 LOOE-16 9.00E-13 2.25E-13 4.20E-15 6.00E-13 1.50E-13
9/29/2003 1.00E-16 9.00E·14 2.25E-14 i3.53E-16 2.00E-14 S.OOE-15 3.32E-16 9.00E·13 2.25E-13 8.69E-15 6.00E-13 L50E-13
12/29/2003 1.02E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.49E-15 9.00E-13 2.25E-13 9.45E-15 6.00E-13 1.50E-13
~2912fl04 l.OOE-16 9.00E-14 2.25E-14 1.26E-16 ~.OOE-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 2.00E-15 6.00E-13 1.50E-13
_6/27/2004 1,00E-16 9.00E-14 2.25E-14 2 53E-16 2.00E-14 5.00E-15 1.00E-16 9,00E-13 2.25E-13 3.23E-15 6.00E-13 1.50E-13
9/27/2004 1.00E-16 9.00E-14 2.25E-14 1.15E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 9,68E-15 6.00E-13 1.50E-13
12/27/2004 1.00E-16 9.00E-14 2.25E-14 2.30E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.37E-14 6.00E-13 1.50E-13
3/28/2005 1.00E-16 9.00E-14 2.25E-14 2.66E-16 2.00E-14 5.00E-15 3.15E-16 9.00E-13 2.25E-13 9.22E-15 6,00E-13 1.50E-13
6/29/2005 1.47E-16 9.00E-14 2.25E-14 1.45E-15 2,00E-14 5.00E-15 l.42E-16 9.00E-13 2.25E-13 9.34E-15 6.00E-13 1.50E-13
9/26/2005 .2.01E-16 9.00E-14 2.25E-14 2.06E-16 2,00E-14 5.00E-15 4.80E-16 9.00E-13 2,25E-13 2.12E-14 6.00E-13 1.SOE-13
1/3/2006 4.54E-16 9.00E-14 2.25E-14 1.24E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 3,60E-14 6.00E-13 1.SOE-13
4/3/2006 1,99E-16 9,00E-14 2.25E-14 1.32E-16 2.00E-14 S.OOE-15 1,00E-16 9.00E-13 1.25E-13 8.36E-15 6,00E-13 1.50E-13
7}3/2006 2.76E-16 9,00E-14 2.25E-14 2.63E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 ;1.25E-13 1.03E-14 6.00E-13 1.50E-13
10/2/2006 4.97E-16 9.00E-14 2.25E-14 2.37E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 1.60E-14 6.00E-13 l.50E-13
1/1/2007 6.46E-16 9.00E-14 2.25E-14 2.81E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 2.10E-14 6.00E-13 1.50E-13
4/2/2007 7,08E-16 9.00E-14 2.25E-14 3.20E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 1 54E-14 6.00E-13 l.50E-13
7/2/2007 9.41E-16 9.00E-14 2.25E-14 1.46E-16 2.00E-14 S.OOE-15 1.99E-16 9,00E-13 2.25E-13 2.56E-14 6,00E-13 1.50E-13
9/30/2007 3.30E-16 9.00E-14 2.25E-14 5.50E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.57E-15 6.00E-13 1.50E-13
12/31/2007 1.42 E-15 9,00E-14 2.25E-14 l.OOE-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 9.93E-15 6.00E-13 1,50E-13
3/31/2008 1.25E-16 IJ.OOE-14 2,25E-14 7.72E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 4.09E-15 6.00E-13 1.50E-13
6/30)2008 1.28E-15 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 3,61E-16 9.00E-13 2.25E-13 1.18E-14 6.00E-13 1.50E-13
--~
Date Effluent Concentration Limit-9E-14 uCi/ml BHV-4U Effluent Concentration Limit-2E-14 uCi/ml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit= 6E-13 uCi/ml BHV-4PB
ALARA Goal = 2.25E-14 uCi/ml ALARAGoal = .SE-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml
Pre 1994 MPC Limit = SE-12 uCi/ml Pre1.9S4 MPC Umlt :c SE-14 uCi/ml Pre 1994 MPC Limit -2E-12 uCi/ml Pre 1994 MPC limit= 4E-12 uCi/ml
Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 A LARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL= 1E-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
9/30/2008 2.72E-15 ~.OOE-14 2.25E-14 1.27E-15 2.00E-14 5.00E-15 7.66E-16 9.00E-13 2.25E-13 1.10E-14 6.00E-13 1.50E·13
12/31/2008 2.88E·15 9.00E-14 2.25E-14 1.10E-15 2.00E-14 5.00E-15 6.56E-16 9.00E-13 2,25E-13 1.38E-14 6.00E-13 1.50E-13
3/15/2009 1.56E-15 9.00E-14 .2.25E-14 4.57E-16 Z.OOE-14 5.00E-15 2.99E-16 9.00E-13 2,25E-13 4,97E-15 G.OOE-13 1.SOE-13
6/15/2009 5.67E-17 9.00E-14 .2.25E-14 2.17E-16 Z.OOE-14 5.00E-15 1.51E-16 9.00E-13 2.25E-13 4.47E-15 6.00E-13 1.50E-13
9/15/2009 4.05E-15 9.00E-14 2.25E-14 1.45E-15 2.00E·14 5.00E-15 2.52E-16 9.00E-13 2.25E-13 1.24E-14 G.OOE-13 1.50E-13
12/15/2009 6.50E-15 9.00E-14 2.25E-14 3.48E-16 2.00E-14 5.00E-15 1.33E-16 9.00E-13 2.25E-13 7.60E-15 G.OOE-13 1.50E-13
3/31/2010 6.01E-15 9.00E-14 2.25E-14 1,26E-16 2.00E-14 5.00E-15 1.34E-16 9.00E-13 2.25E-13 1.19E-14 6.00E-13 1.50E-13
6/30/2010 2.33E-15 9.00E-14 2.25E-14 7.29E-16 2.00E-14 5.00E-15 2.66E-16 9.00E-13 2.25E-13 3.27E·15 G.OOE-13 1.50E·13
9/30/2010 4.77E·15 9.00E·14 2,25E·14 1.80E·15 2.00E·14 5.00E-15 8.23E-16 !J.OOE-13 .2.25E·13 S.llE-15 6.00E-13 1.SOE-13
12/31/2010 3.93E·15 9.00E·14 2,25E-14 3.90E-16 2.00E·14 S.OOE-15 2.56E-16 9.00E-13 2.25E-13 1.13E-14 6.00E·13 1.SOE·13
4/4/2011 1.29E-15 9.00E-14 2.25E·14 1.40E-16 2.00E·14 S.OOE-15 11.58E-16 9.00E-13 2.25E-13 1.11E-14 b.OOE-13 1.50E·13
7/4/2011 3.30E-15 9.00E-14 2.25E-14 5.44E-16 2.00E·14 5.00E-15 4.18E-16 9,00E-13 2.25E-13 8,26E-15 6.00E·13 1.SOE·13
10/3/2011 1.32E·15 9.00E·14 2.25E·14 7.89E-16 2.00E·l4 S.OOE-15 1.28E-16 9.00E-13 2.25E-13 1.18E-14 6.00E-13 l.SOE-13
1/3/2012 1.04E·15 9.00E·14 2.25E·14 3.25E-16 2.00E·14 5.00E-15 2.28E-16 9,00E-13 2.25E-13 1.14E·14 6.00E-13 1.50E-13
4/3/2012 2.51E·15 9.00E-14 2.2SE·14 5.02E·16 2.00E·14 5.00E-15 2.27E-16 9.00E·13 2.25E-13 1.03E·14 p.OOE-13 1.50E-13
7/2/2012 2.62E-15 9,00E-14 2.25E-14 1.23E-15 2.00E·14 5,00E·15 2.97E-16 9.00E·13 2.25E-13 9.27E·15 6.00E-13 1.50E·13
10/1/2012 4.05E·15 9.00E-14 2.25E·14 8.33E-16 2.00E·14 5.00E-15 5.43E-16 S.OOE-13 2.25E-13 1.21E-14 6.00E-13 1.50E·13
12/31/2012 2.32E·15 9.00E-14 2.25E-14 5.89E-16 2.00E·14 S.OOE-15 3.75E-16 9.00E-13 2.25E·13 1.56E·14 6.00E-13 l.SOE-13
3/25/2013 3.04E·15 9.00E·14 ?.25E-14 4.99E-16 2.00E·14 S.OOE-15 2.79E·16 9.00E-13 2~5E-13 2 13E·14 6.00E-13 l.SOE-13
7/2/2013 2.SOE·15 9.00E-14 2.25E-14 3.62E-16 2.00E·14 5,00E·15 2.40E·16 9.00E·13 2.25E·13 4.93E·15 6.00E-13 1.50E·13
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TABS
BHV -5 AIR SAMPLING GRAPHS AND DATA TABLE
Date Eflluent Concentration limit= SE-14uG/ml BHV-SU Effluent Concentration limit-2E-14 uCi/ml BHV-ST Effluent Concentration limit= 9E-13 uCi/ml BHV-SR Effluent Concentration limit= 6E-13 uCi/ml BHV..SPB
AlARA Goal = 2.25E-14 ul;i/ml ALARA Goal-SE-13 uCl/nil AlARAGoal-2.25E-13 uCi/ml ALARA Goal= l.SE-13 11Ci/ml
Pre 1994 MPC limit= SE-12 ud/ml Prel.!l94 MPC limit"" !JE-1.4 uCI/ml' Pre 1994 MPC limit= 2E-12 uCi/ml Pre 1994 MPC limit= 4E-12 uCi/ml
Pre 1994 A lARA GOAL= 1.25E-12 uCI/ml Pre 1994 ALARA GOAL= SE-13 uCi/ml Pre 1994 ALARA GOAL= 1E-12 uCi/ml
Coil" EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFC A
gnsri!lsl 2.44E-15 S.OOE-12 1.25E-12 1.53E-15 S.OOE-14 2.00E-14 7.54E-16 2,00E-12 5.00E-13 1.69E-14 4.00E-12 l.OOE-12
12/14/1981 4.84E-15 S.OOE-12 1.25E-12 V~lS 8.00E-14 2.00E-14 1.84E-15 2.00E-12 5.00E-13 1.53E-14 4.00&12 l.OOE-12
3!29/1982: 1.04&15 S.OOE-12 1.25E-12 2,62E-15 8.00E-14 2.00E-14 1.11E-15 2.00E-12 5.00E-13 2.98E-14 4.00E-12 l.OOE-12
11/30/19~ .i.61E-15 5.00E-12 1.25E-12 7.61E-15 8.00E-14 2.00E-14 1.39E-15 2.00E-12 S,OOE-13 1.80E-15 4.00E-12 1 OOE-12
9/27/1982 1.71E-14 S.OOE-12 1.25E-12 9.46E-15 8.00E-14 2.00E-14 3.80E-15 Z.OOE-12 S.OOE-13 ~.3SE·14 4.00E-12 l.OOE-12
1/3}1.983 1.90E-14 S.OOE-12 1.25E-12 5.77E-15 8.00E-14 Z.OOE-14 9.34E-17 2.00E-12 S.OOE-13 4.32E-14 4.00E-12 1.00&12
4/4/1.983 5.00E-12 1.25E-12 2.33E-15 8.00E-14 Z.OOE-14 5.93E-16 2.00E-12 5.006·13 3.ait-t.4 ~.D0(-12 1.00&1.2
6/3Dil.983 7.62E-16 5.00E-12 1.25E-12 .3.25E-15 8.00E-14 2.00E-14 6.28E-15 2.00E-12 5.00E-13 2.69E-14 4,0QE·12 UlOE-Ii
10/3/1983 4.26E-16 5.00E-12 L25E-12 l.lOE-15 S.OOE-14 2.00E-14 3.63E-16 2.00E-12 5.00E-13 2.08E-14 !l--OOE-12 LOOE-1.2
1/3/1984 6,96E-15 S.OOE-12 1.25E-12 9.69E-16 8.00E-14 2.00E-14 9,60E-16 2.00E-12 5.00E-13 1.83E-14 4.00E-12 l.OOE-12
4/2/liJ$4 1.64E-15 S.OOE-12 1.25E-12 1.34E-15 B.OOE-14 2.00E-14 3.88E-15 2.00E-12 5,00E-13 4,67E-14 4 OOE-12 l.OOE-12
7/2/1984 1.12E-15 S.OOE-12 1.25E-12 1.92E-15 8.00E-14 2.00E-14 3.31E-15 2.00E-12 5.00E-13 2.21E-14 4.00E-12 l.OOE-12
10/1/1984 1.11E-15 5.00E-12 1.25E-12 3.13E-16 8.00E-14 2.00E-14 4.21E-16 2.00E-12 5.00E-13 1.57E-14 4.00E-12 LOOE-12
1!2/1985 7.32E-16 5,00E-12 1.25E-12 6.71E-16 8.00E-14 2.00E-14 4.94E-16 2.00E-12 S.OOE-13 2.42E-14 4.00E-~ 1.00E-12
4/1/1985 2.36E-16 5.00E-12 1.25E-12 5.43E-16 8.00E-14 2.00E-14 2.71E-16 Z.OOE-12 5.00E-13 1.25E-14 4.00E-12 l.OOE-12
7/~MBS 7.58E-16 5.00E-12 1.25E-12 4.00E-16 8.00E-14 2.00E-14 6.90E-16 2,00E-12 S.OOE-13 2.15E-14 4.00E-12 1.00E-12
9/.30}1985 7.47E-15 5,00E-12 1.25E-12 1.16E-15 8.00E-14 2.00E-14 2.19E-15 2.00E-12 5.00E-13 9.20E-15 4.00E-12 l.OOE-12
1/2/1986 1.75E-14 5.00E-12 1.25E-12 7.24E-15 8.00E-14 2.00E-14 3.83E-15 2,00E-12 5 OOE-13 1.13E-16 4.00E-12 l.OO.E.-12 '
4/1/1986 2.99E-14 5.00E-12 1.25E-12 7.64E-15 B.OOE-14 2.00E-14 1.51E-14 2.00E-12 5.00E-13 2.22E-14 4.00E-12 I,OOE-12 I
6/30/1986 2.23E-14 S.OOE-12 1.25E-12 5.19E-15 8.00E-14 2.00E-14 1.05E-14 2.00E-12 5.00E-13 2.16E-14 <l.OOE-12. l.OOE-12
10/27/1986 2.33E-1~ :S.OOE-12 1.25E-12 7.78E-15 il.OOE-14 2.00E-14 1.60E-14 2.00E-12 5.00E-13 2,02E-14 4.00E-12 1 OOE-12
12/lS/1985 3.40E-14 .S.OOE-12 1.25E-12 5.35E-15 8.00E-14 2.00E-14 1.47E-14 2.00E-12 5.00E-13 2.82E-14 4.00E-12 l.OOE-12 I
3/16/1'1'07 2.06E-14 S.OOE-12 1.25E-12 4.50E-15 8,00E-14 2.00E-14 6.74E-15 2.00E-12 5.00E-13 7,29E-14 4.00E-12 l.OOE-12
5/11/1987 2.50E-14 5.00E-12 1.25E-12 8.54E-15 8.00E-14 2.00E-14 B.15E-15 Z.OOE-12 6.00E-13 3.28E-14 4 OOE-12 l.OOE-12
9'l9/1987 2.6SE·l<l 5,00E-12 1.25E-12 6.62E-15 8.00E-14 2.00E-14 9.34E-15 Z.OOE-12 5.00E-13 2.77E-14 4.00E-12 l.OOE-12
un/-1987 LSOE-14 5.00E-12 1.25E-12 7.09E-15 S.OOE-14 Z.OOE-14 7.20E-15 2.00E-12 5.00E-13 L77E-14 4.00E-12 1,00E-12
2/16/1988 1.01E-14 5.00E-12 1.25E-12 2.98E-15 8.00E-14 Z.OOE-14 3.93E-15 2.00E-12 5.00E-13 3.36E-14 4.00E-12 1.00E-12
5/113/19!1& 1.78E-14 5.00E-12 1.25E-12 8.14E-15 8.00E-14 2.00E-14 7.43E-15 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 l.OOE-12
6/15/1988 1.79E-14 5.00E-12 1.25E-12 1.49E-14 8.00E-14 2.00E-14 5.34E-15 2.00E-12 5.00E-13 2.45E-14 4.00E-12 l.OOE-12
U/14/1988 4.46E'·14 S.OOE-12 1.25E-12 1.39E-14 8.00E-14 2,00E-14 1,17E-14 2.00E-12 5.00E-13 3.43E-14 4.00E-12 l.OO.E-U
2/13/1969 1.67E-14 S.OOE-12 1.25E-12 5.54E-15 S.OOE-14 2.00E·14 7.20E-15 2,00E-12 5.00E-13 5,02E-14 4.00E-12 l.OOE-12
5/15}1989 2.03E-14 p.OOE-12 1.25E-12 7.05E-15 S.OOE-14 2.00E-14 9.56E-16 2.00E-12 5.00E-13 1.43E-14 4.00E-12 1.00E-12
8/l<l/'1989 2.81E-15 5.00E-12 1.25E-12 3,78E-15 S.OOE-14 2.00E-14 9.26E-15 2.00E-12 S.OOE-13 1.50E-14 4.00E-12 l.OOE-12 i
11/13/1989 5.38E-14 5.00E-12 1.25E-12 8.01E-15 S.OOE-14 2.00E-14 1.81E-14 2.00E-12 5.00E-13 4,09E-14 4.00E-12 l.OOE-12
2/l2/1.99Q USE-14 5.00E-12 1.25E-12 1.48E-14 S.OOE-14 ~.OOE-14 1.28E-14 2.00E-12 5.00E-13 3.88E-14 4.00E·12 l.OOE-12
S/1'l/1991l 2.18E-14 5.00E-12 1.25E-12 1.70E-14 S.OOE-14 2.00E-14 1.59E-14 Z.OOE-12 S.OOE-13 3.49E-14 4.00E-12 l.OOE-12
8/13/1.990 9.53E-15 5,00E-12 1,25E-12 l.lOE-14 8.00E-14 ~.OOE-14 3.27E-15 2,00E-12 'S.OOE-13 1.27E-14 4.00E-12 1.00E-12
ll/12/i.99o 1.11E-14 S.OOE-12 1.25E-12 5.27E-15 8.00E-14 2.00E-14 S,38E-15 2.00E-12 S.OOE-13 1.56E-14 4,00E-12 l.OOE-12
2/lli1991 6.35E-16 5.00E-12 1.25E-12 3.13E-16 8.00E-14 2.00E-14 2.31E-16 2.00E-12 5.00E-13 3.89E-14 4.00E-12 l.OOE-12
5/13/I'JlU 122E-15 5.00E-12 1.25E-12 6.14E-15 S.OOE-14 2.00E-14 4.41E-15 2.00E-12 5.00E-13 2,50E-14 4.00E-12 l.OOE-12
8/12f199l 7.84E-16 S.OOE-12 1.25E-12 1,43E-15 8.00E-14 2.00E·14 4.47E-16 2.00E-12 5.00E-13 1.84E-14 4.00E-12 1.00E-l1
11/11/1991 5.37E-16 5.00E-12 L25E-12 4.20E-16 S.OOE-14 2.00E-14 1.37E-16 2.00E-12 5,00£-13 1,27E-14 4.00E·12 1.00E-12
2/10/1992 3.54E-16 S.OOE-12 1.25E-12 1.18E-16 S.OOE-14 Z.OOE-14 4.08E-17 2.00E-12 5.00E-13 3.69E-14 4.00E·12 1,00E-12
5/11/1992 4.71E-16 5.00E-12 1.25E-12 9.58E-16 8 OOE-14 2.00E-14 8.31E-17 2.00E-12 5.00E-13 1.43E-14 4.00E-12 1.00E-12
8/10/1992 5.32E-15 5.00E-12 1.25E-12 3.36E-16 S.OOE-14 2.00E-14 1.65E-16 2.00E-12 5,00E-13 1.59E-14 4.00E-12 1,00E-12
11/9/1992 3.66E-16 5.00E-12 1.25E-12 2.25E-16 8.00E-14 2.00E-14 1.08E-16 l.OOE-12 6.00E-13 2.24E-14 4.00E-12 1,00E-12
2/$/199~ 2.05E·16 5.00E-12 1.25E-12 9.14E-17 8,00E-14 2.00E-14 6.31E-17 Z.OOE-12 S.OOE-13 3.41E-14 4.00E-12 1,00E-12
5/·10/1993 4,80E-16 5,00E-12 1.25E-12 8.25E-16 8.00E-14 2.00E·14 1.26E-15 2.00E-12 5.00E-13 1.83E-14 4.00E-12 l.OOE-12
8/10/1.993 8.30E-16 5.00E-12 1.25E-12 1.90E-16 8.00E-14 2.00E-14 2.10E-16 2.00E-12 5.00E-13 1.70E-14 4.00E-12 l.OOE-12
li/S/1.993 2.70E-16 5.00E-12 1.25E-12 S.OOE-17 8.00E-14 2.00&.14 7.00E-17 2.00E-12 S.OOE-13 2.34E-14 4.00E-12 l.OOE-12
211/!!YJ4 3.18E-16 S.OOE-12 1.25E-12 l.OOE-16 8 OOE-14 2.00E·14 5.18E-16 2.00E-12 5.00E-13 3.64E-14 4.00E-12 l.OOE-12
S/9/1~ l.SOE-15 S.OOE-12 1.25E-12 9.78E-16 8.00€-14 2.00E-14 l.lOE-15 2,00E-12 5.00E-13 8 30E-15 4.00E-12 1.00E-12
8/9/1994 2.67E-15 5.00E-12 1.25E-12 1.11E-15 a.ooe-t<~ 2.00E-14 4.9SE·16 2.00E-12 5.00E-13 l.OOE-16 4.00E-12 l.OOE-12
11/7/1994 9.21E-17 5.00E-12 1.25E-12 1.59E-15 S.OOE-14 2.00t-l.4 1.66£·15 2.00€-12 5.00~-13 l..OOE-16 4.00E-12 1,00E-12
Date Effluent Concentration Limit -9E-14 uCi/ml BHV-SU Effluent Concentration Limit -2E-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit= 6E-13 uCi/ml BHV-SPB
ALARAGoal = :Z.25E-14 uCi/ml AlARA Goal= SE-13 uCi/ml AlARAGoal = 2.2SE-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml
Pn! 1994 MPC Limit = SE-12 uCi/ml Pre 199<1 MPG lfl'lllt= BE-14 uCi/ml Pr!!].994 MPC Umfl= 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml
'Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml pre 1994 ALARA GOAL = SE-13 uCi/ml pre 1994 A LARA GOAL= 1E-12 uCi/ml
t one EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
2/7/1995 1.51E-15 9.00E-14 2.25E-14 9.50E-16 2.00E-14 5.00E-15 9.70E-17 9.00E-13 2.25E-13 9.35E-15 6.00E-13 1.SOE-13
5/9/1995 2.21E-16 9,00E-14 2.25E-14 8.56E-16 2.00E-14 5.00E-15 3.06E-15 9.00E-13 2.25E-13 4.34E-15 p.OOE-13 1.50E-13
8/9/1995 1.66E-16 9,00E-14 2.25E-14 1.67E-15 2.00E-14 S.OOE-15 3,90E-15 9.00E-13 2.25E-13 S.60E-15 6.00E-13 1.50E-13
11/11/1995 2.04E-14 9.00E-14 2.25E-14 6.70E-15 2.00E-14 5.00E-15 7.65E-15 9.00E-13 2.25E-13 4.47E-15 6.00E-13 1.50E-13
2/5/1996 4.50E-14 9.00E-14 2 25E-14 3.58E-14 2.00E-14 S.OOE-15 2.39E-14 9.00E-13 2,25E-13 7.30E-15 6.00E-13 1.50E-13
5/6/1996 1.76E-15 9.00E-14 2.25E-14 3.57E-15 2.00E-14 S.OOE-15 9.55E-16 9.00E-13 2.25E-13 7.54E-15 6,00E-13 1.SOE-13
8/5/1996 2.37E-15 9,00E-14 2.25E·14 8.18E-15 2.00E-14 S.OOE-15 7,46E-16 9.00E-13 2.25E-13 5.75E-15 6.00E-13 1.50E-13
11/6/1996 3.53E-15 9.00E-14 2.25E-14 5.31E-15 2.00E-14 5.00E-15 9,39E-16 9,00E-13 2.25E-13 1.21E-14 G.OOE-13 l.SOE-13
2/6/1997 1.84E-16 9.00E-14 2.25E-14 2.01E-16 2.00E-14 5.00E-15 1.87E-16 9.00E-13 2.25E-13 6.14E-15 6.00E-13 1.50E-13
5/5/1997 5.75E-16 9.00E-14 2.25E-14 7.24E-16 l,OOE-14 5.00E-15 6.07E-16 9.00E-13 2.2SE-13 4.75E-15 6.00E-13 1.50E-13
.8/11/1997 1.21E-15 9,00E-14 2.25E-14 7.39E-16 2.00E-14 5.00E-15 5.05E-16 9.00E-13 2.25E-13 4.92E-15 6,00E-13 1.50E-13
1/5/1998 9.89E-16 9.00E-14 2.25E-14 1.92E-15 2.00E-14 5.00E-15 6.21E-16 9.00E-13 2.25E-13 4.68E-15 6.00E-13 1.50E-13
4/28/1998 2,84E-15 9.00E-14 2.25E-14 2.38E-15 2.00E-14 5.00E-15 1.72E-15 9.00E-13 2.25E-13 7.35E-15 6.00E-13 1.50E-13
7/3l/19'J8 7.49E-16 9.00E-14 2.25E-14 1.49E-15 2.00E-14 5,00E-15 8.34E-16 9.00E-13 2.25E-13 7.01E-15 6.00E-13 1,50E-13 !
9/28/1998 1.07E-15 9.00E-14 2.25E-14 9.20E-16 2.00E-14 S,OOE-15 6.32E-16 9.00E-13 2.25E-13 3.95E-15 6,00E-13 1,50E-13 I
12/28/1998 8.51E-15 9.00E-14 2.25E-14 4.58E-15 2.00E-14 5.00E-15 4.58E-15 9.00E-13 2,25E-13 1.43E-14 6.00E-13 1.50E-13 I
3/29/1999 3.75E-15 S.OOE-14 2.25E-14 2.45E-15 2.00E-14 5.00E-15 239E-15 9.00E-13 2.25E-13 8.46E-15 6.00E-13 1.50E-13
7/3/1999 1.53E-15 9,00E-14 2.25E-14 8.65E-16 2.00E-14 5.00E-15 5.52E-16 9.00E-13 2.25E-13 7.20E-15 6.00E-13 1.50E-13 ,
9/27/1999 5.83E-15 S.OOE-14 2.25E-14 3,52E-15 2.00E-14 5.00E-15 2.55E-15 9,00E-13 2.25E-13 8.22E-15 G.OOE-13 1.50E-13 1
12/28/1999 9.48E-15 9.00E-14 2.25E-14 6.20E-15 2.00E-14 5,00E-15 3.96E-15 9.00E-13 2.25E-13 7.56E-15 6.00E-13 1.50E-13
3/27/2000 2.06E-15 9.00E-14 2.25E-14 1.27E-15 2.00E-14 S.OOE-15 1.09E-15 9.00E-13 2.25E-13 7.72E-15 6.00E-13 1,50E-13
6/26/2000 1,50E-15 9,00E-14 2.25E-14 1.24E-15 2.00E-14 li.OOE-15 1.01E-15 S.OOE-13 2.25E-13 4.36E-15 6.00E-13 1.50E-13
9j 26/2000 1.04E-15 9.00E-14 2.25E-14 5.45E-16 2.00E-14 S.OOE-15 6.01E-16 9.00E-13 2.25E-13 7.67E-15 p.OOE-13 1.SOE-13
12/26/2000 1.48E-15 9.00E-14 2.25E-14 7.56E-16 2.00E-14 G.OOE-15 6.84E-16 S.OOE-13 2.25E-13 ?.OOE-15 6,00E-13 1.50E-13
3/26/2001 4.27E-16 9.00E-14 2.25E-14 2.19E-16 2.00E-14 S.OOE-15 1.89E-16 9.00E-13 2.25E-13 6.13E-15 6.00E-13 1.50E-13
7/2/2001 4.52E-16 9.00E-14 2.25E-14 4.02E-16 Z.OOE-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 7.48E-15 p.OOE-13 1.50E-13 i
9/24/2001 4.65E-16 9,00E-14 2.25E-14 2.06E-16 2.00E-14 S.OOE-15 2.02E-16 9.00E-13 2.25E-13 6.98E-15 6.00E-13 1.50E-13 '
12/31/2001 7.40E-16 9.00E-14 2.25E-14 3.51E-16 2.00E-14 S.OOE-15 3,64E-16 9.00E-13 2.25E-13 4.72E-15 6.00E-13 1.50E-13
4/1/2002 1.26E-15 9.00E-14 2.25E-14 '7.53E-16 2.00E-14 5.00E-15 7.19E-16 9.00E-13 2.25E-13 9.65E-15 G.OOE-13 1.50E-13
7/1/2002 1.02E-15 9.00E-14 2.25E-14 1.03E-15 2.00E-14 5.00E-15 3.39E-16 9.00E-13 ~.25E-13 7.20E-15 6.00E-13 1.50E-13
9/30/2002 5.82E-16 9.00E-14 2.25E-14 9.28E-16 2.00E-14 5.00E-15 3.14E-16 9.00E-13 2.25E-13 4.48E-15 G.OOE-13 1.50E-13
12/30/2002 l.OOE-16 9.00E-14 2.25E-14 7.67E-16 2.00E-14 S.OOE-15 3.48E-16 9.00E-13 2,25E-13 9.56E-15 6.00E-13 1.50E-13
3/31/2003 1.13E-15 9.00E-14 2.25E-14 7.41E-16 2.00E-14 5.00E-15 4.41E-16 9.00E-13 2.25E-13 6.68E-15 6.00E-13 1.SOE-13
6/30/2003 4,35E-16 9.00E-14 2.25E-14 5.08E-16 l.OOE-14 5.00E-15 2.51E-16 9.00E-13 2.25E-13 1.34E-15 6,00E-13 1.50E-13 !
9/~2003 1.51E-16 9.00E-14 2.25E-14 1.02E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.28E-15 6.00E-13 1.50E-13 I
12/29/2003 1.52E-16 9.00E-14 2.25E-14 1.54E-16 Z.OOE-14 5.00E-15 1.51E-16 9.00E-13 2.25E-13 7.02E-15 6.00E-13 1.50E-13
3/29/2004 l.OOE-16 9.00E-14 2.25E-14 1.12E-16 2.00E-14 5,00E-15 l.OOE-16 9.00E-13 2.25E-13 8,82E-15 6.00E-13 1.50E-13
6/27/2004 1.18E-16 9,00E-14 2.25E-14 3.11E-16 2.00E-14 5.00E-15 1.25E-16 9.00E-13 2.25E-13 2.47E-15 6.00E-13 1.50E-13
9/27/2004 1.16E-16 9.00E-14 2.25E-14 1.72E-16 2.00E-14 5.00E-15 1.18E-16 9.00E-13 2.25E-13 l.lOE-14 6 OOE-13 1.50E-13
12/27/2004 L14E-16 9.00E-14 2.25E-14 1.06E-16 2,00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 1.59E-14 6,00E-13 1.50E-13 '
3/28}2005 l.OOE-16 9.00E-14 2.25E-14 2.04E-16 2.00E-14 5.00E-15 1.83E-16 9.00E-13 2.25E-13 8.57E-15 6.00E-13 1.50E-13
6/29/2005 1.83E-16 9.00E-14 2.25E-14 3.81E-16 2.00E-14 5.00E-15 3.09E-16 9.00E-13 2.25E-13 l.OGE-14 G.OOE-13 1.50E-13
9/26/2005 2.87E-16 9.00E-14 2.25E-14 8.21E-16 2.00E-14 5.00E-15 3.71E-14 9.00E-13 2.25E-13 6.28E-14 6.00E-13 1.50E-13
1/3/2006 8.74E-16 9 OOE-14 2.25E-14 3.79E-16 2.00E-14 G.OOE-15 1.31E-16 9.00E-13 2.25E-13 4.32E-14 6.00E-13 1.50E-13
4/3/2006 5.22E-16 9.00E-14 2.25E-14 6,66E-16 2.00E-14 S.OOE-15 l.llE-16 .9.00E·l3 2.25E-13 9.34E-15 6.00E-13 1.50E-13
7/3/2006 3.08E-16 9.00E-14 2.25E-14 1,10E-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 1.25E-14 G.OOE-13 1.50E-13
10/2/2006 9.14E-16 9.00E-14 2.25E-14 4.95E-16 2.00E-14 S.OOE-15 1.86E-16 9.00E-13 2.25E-13 1.67E-14 6.00E-13 1.50E-13
1/1/2007 9,49E-16 9.00E-14 2.25E-14 6.81E-16 2.00E-14 '5.00E-15 2.02E-16 9.00E-13 2,25E-13 1.31E-14 6.00E-13 1,50E-13 I
4/2/2007 1.08E-15 9.00E-14 2.25E-14 8.22E-16 2.00E-14 5.00E-15 2.26E-16 9.00E-13 2.25E-13 1.64E-14 6,00E-13 l.SOE-13
7/2/2007 1.54E-15 9.00E-14 2,25E-14 8.16E-16 2.00E-14 5.00E-15 4.76E-16 9.00E-13 2.25E-13 2.12E-14 6,00E-13 1.50E-13
9/30/2007 4.90E-16 9.00E-14 '2.25E-14 2.37E-16 2.00E-14 S.OOE-15 l.OOE-16 9,00E-13 2.25E-13 6,65E-15 6.00E-13 1.50E-13
12/31/2007 1.46E-15 9.00E-14 2.25E-14 S.67E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.02E-14 6.00E-13 1.50E-13
3/31/2008 3.16E-16 9.00E-14 2.25E-14 6.17E-16 2.00E-14 S.OOE-15 3.71E-16 9.00E-13 2.25E-13 4.82E-15 6 OOE-13 1.50E-13
6/30/2008 3.13E-15 9.00E-14 2.25E-14 l.SSE-15 2.00E-14 S.OOE-15 9.27E-16 9.00E-13 2.25E-13 7.40E-15 6 OOE-13 1.50E-13
Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-SU Effluent Concentration limit= 2E-14 uCi/ml BHV-ST Effluent Concentration Limit= 9E-13 uCi/ml BHV-SR Effluent Concentration limit= 6E-13 uCi/ml BHV-SPB
ALARAGoal = 2.25E-14 uCi/ml ALARA Goal= SE-13 uCifml ALARA Goal= .Z.ZSE-13 uCi/ml ALARAGoal = 1.5E-13 uCi/ml
pre 1994 MPC limit-SE-12 uCi/ml Pre 1994 MPC Limit-BE-14 uCi/ml Pre 1994 MPC Limit= ZE-12 uCi/ml Pre 1.994 MPC.I,Imlt= 4E-12 uCi/ml
Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 A LARA GOAL = sE-13 uCi/ml pre 1994 ALARA GOAL = l E-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
9/30/2008 7.08E-15 9.00E-14 2.25E-14 3.41E-15 2.00E-14 S.OOE-15 2.52E-15 9.00E-13 2.25E-13 1.15E-14 6.00E-13 1.50E-13
12/31/2008 7.22E-15 9.00E-14 2.25E-14 2.82E-15 2.00E-14 S.OOE-15 3.03E-15 9.00E-13 2.25E-13 1.59E-14 G.OOE-13 1.SOE-13
3/15/2009 4.13E-15 9.00E-14 2.25E-14 1.39E-15 2.00E-14 S.OOE-15 1.41E-15 9.00E-13 2.25E-13 4.66E-15 6.00E-13 l.50E-13
6/15/2009 2.31E-16 9.00E-14 2.25E-14 7.79E-16 2.00E-14 S.OOE-15 6.37E-16 9.00E-13 2.25E-13 4.18E-15 6.00E-13 1.50E-13
'J/15/2009 3.10E-15 9.00E-14 2.25E-14 9.20E-16 2.00E-14 S.OOE-15 6,36E-16 9.00E-13 2.25E-13 121E-14 6.00E-13 1.50E-13
12/15/2009 5.77E-15 9.00E-14 :2.25E-14 3.13E-16 .2.00E-14 S.OOE-15 1.92E-16 9.00E-13 2,25E-13 2.48E-15 6.00E-13 1.50E-13
3/31/2010 4.78E-15 9.00E-14 ,2.25E-14 ,3.73E-16 .2.00E-14 5,00E-15 4.19E-16 9.00E-13 2,.25E-13 1.30E-14 G.OOE-13 1.50E-13
6/30/2010 4.35E-15 9.00E-14 .2.25E-14 7.84E-16 2.00E-14 S.OOE-15 1.05E-15 9.00E-13 2.25E-13 4.40E-15 G,OOE-13 1.50E-13
9/30/2010 3.57E-15 IJ.OOE-14 2.25E-14 1.14E-15 2.00E-14 5.00E-15 7.97E-16 9.00E-13 2.25E-13 3.78E-15 6.00E-13 1.50E-13
12/31/2010 8.52E-15 9.00E-14 2.25E-14 1.45E-15 2.00E-14 5.00E-15 1.29E-15 9.00E-13 2,25E-13 1.33E-14 6.00E-13 1.50E-13
M4/20n 3.20E-15 9.00E-14 2.25E-14 8.89E-16 2.00E-14 5.00E-15 1.10E-15 9.00E-13 2,25E-13 1.48E-14 6.00E-13 1.50E-13
7/4/2011 6.98E-15 9.00E-14 2.25E-14 2.03E-15 2.00E-14 5.00E-15 2.52E-15 9.00E-13 2,25E-13 l.OSE-14 6,00E-13 1.50E-13
10/3/2011 3.11E-15 9.00E-14 2.25E-14 1.14E-15 2.00E-14 S.OOE-15 5.75E-16 9.00E-13 2.25E-13 1.41E-14 6.00E-13 1.50E-13
1/3/2012 4.44E-15 9.DDE-14 2.25E-14 2.14E-15 2.00E-14 S.OOE-15 1.53E-15 9.00E-13 2.25E-13 2.0SE-14 6.00E-13 l.SOE-13
4/3/2012 5.52E-15 9.00E-14 2.25E-14 3.24E-15 2.00E-14 5.00E-15 1.79E-15 9.00E-13 2.25E-13 1.55E-14 G.OOE-13 1.50E-13
7f2j2012 5.87E-15 I).OOE-14 2,25E-14 3.06E-15 2.00E-14 5.00E-15 1.21E-15 9.00E-13 .2.25E-13 l.llE-14 6.00E-13 1.50E-13
10/1/2012 6.73E-15 9.00E-14 2.25E-14 2.59E-15 2.00E-14 S.OOE-15 2.43E-15 9.00E-13 :2.25E-13 l,30E-14 6.00E-13 1.50E-13
12/31/2012 4.50E-15 9.00E-14 2.25E-14 1.62E-15 2.00E-14 S.OOE-15 1.79E-15 9.00E-13 .2.25E-13 1.74E-14 6.00E-13 l.SOE-13
3/25/2013 6.66E-15 9.00E-14 2.25E-14 1.48E-15 2.00E-14 S.OOE-15 1.12E-15 9.00E-13 2.25E-13 l.BOE-14 p.OOE-13 1.50E-13
7/2/2013 7.35E-15 9.00E-14 2.25E-14 1.72E-15 2,00E-14 S.OOE-15 2.02E-15 9.00E-13 2.25E-13 6.67E-15 G.OOE-13 1.50E-13
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TAB6
BHV-6 AIR SAMPLING GRAPHS AND DATA TABLE
I Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-6U Effluent Concentration limit-2E-14 uCi/ml BHV-6T Effluent Concentration Limit= 9E-13 uCi/ml BHV-6R Effluent Concentration Limit = 6E-13 uCi/ml BHV-6PB I
ALARA Goal= 2.25E-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal= 2.25E-13 uCi/ml ALARA Goal= l.SE-13 uCi/ml I Pre 1994 MPC limit= SE-12 uCi/ml Pre 1994 MPC limit= BE-14 uCi/ml Pre 1994 M PC limit = 2E-12 uCi/ml Pr.,J.994 MPC limit=-4E-12 uCi/ml
Pre 1994 ALARA GOAL= 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 A LARA GOAL-lE-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
9/28/1981 S.OOE-12 1.25E-12 8.00E·14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
12/14/1981 S.OOE-12 1.2SE-12 8.00E-14 2,00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
3/29/1982 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E·12 I
6/30/1982 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E·12
9/27/1982 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
1/3/1983 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5,00E-13 4.00E-12 1.00E·12
4/4/1983 5.00E-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E·12
6/30/1983 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5,00E-13 4.00E-12 1.00E-12
10/3/1983 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
1/3/1984 5.00E-12 1.2SE-12 8.00E-14 2.00E-14 2 OOE-12 5.00E-13 4.00E-12 l.OOE-12
4/2/1984 5.00E-12 1.25E-12 8,00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12
7/2/1984 5.00E-12 1,25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE·12
10/1/1984 5,00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12
1/2/1985 5,00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
4/1/1985 5,00E-12 1.25E-12 8.00E-14 2,00E-14 ' 2.00E-12 5.00E-13 4.00E-12 1.00E·12
7/1/1985 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12
9/30/1985 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 i.OOE-12
1/2/1986 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12
4/1/1986 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
6/30/1986 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12
10)27/1986 5.00E-12 1.25E-12 8.00E-14 2,00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
12/15/1986 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
3/16/1987 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
5/11/1987 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
9/9/1987 5,00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
11/2/1987 5,00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
;2/16/1988 5.00E-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
5/18/1988 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4,00E-12 l.OOE-12
8/15/1988 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
11/14/1988 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
2/13/1989 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E·12
5/15/1989 S.OOE-12 1.25E-12 8.00E-14 2,00E-14 2.00E-12 S.OOE-13 4,00E-12 t.OOE-12
8/14/1989 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12
ll/13/1989 5.00E-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
2/12/1990 5.00E-12 1.25E-12 8.00E-14 2,00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12
5/14/1990 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12
8/13/1990 5 OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12
11/12/1990 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
2/11/1991 5.00E-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 LOOE-12
5/13/1991 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
8/12/1991 5.00E-12 1.25E·12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4,00E-12 l .OOE-12
11/11/1991 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE·12
2/10/1992 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
5/11/1992 5,00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l .OOE-12
8/10/1992 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12
11/9/1992 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 LOOE-12
2/9/1993 5.00E-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
5/10/1993 5.00E-12 1.25E-12 S.OOE-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 l.OOE-12
8}10/1993 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 LOOE-12
11/8/1993 S.OOE-12 1.25E-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4,00E-12 l.OOE-12
2/7/1994 5.00E-12 1.25E-12 8 OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
"p/9/1994 S.OOE-12 1.25E-12 S.OOE-14 2.00E-14 2,00E-12 5.00E-13 4.00E-12 l.OOE-12
8/9/1994 S.OOE-12 1 25E-12 8.00E-14 2.00E-14 2,00E-12 5.00E-13 4.00E-12 l.OOE-12
11/7/1994 S.OOE-12 1.25E-12 '-----B.OOE-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 l.OOE-12
Date Effluent Concentration Limit= 9E-14 uCi/ml BHV-6U Effluent Concentration Limit = ZE-14 uCi/ml BHV-6T Effluent Concentration Limit= 9E-13 uCi/ml BHV-6R Effluent Concentration Limit= 6E-13 uCi/ml BHV-6PB
ALARA Goal= 2.25E-14 uCi/ml ALARA Goal-SE-13 uCi/ml ALARAGoal-2.25E-13 uCi/ml ALARA Goal= 1.5E-13 uCi/ml
Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit= BE-14 uCi/ml p;e 1.994 MPC limit = 2E-12 uCi/ml Pre 1994 MPC Limit= 4E-12 uCi/ml
Pre 1994 ALARA GOAL= 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = ISE-13 uCi/ml pre 1994 A LARA GOAL= 1E-12 uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
2/7/1995 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13
5/9/1995 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13
8/9/1995 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13
11/11/1995 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 B.OOE-13 2.25E-13 6.00E-13 1.50E-13
2JS/l!f95 9,00E-14 2,25E-14 2.00E-14 S,OOE-15 g,ooe.-13 2.25E-13 .G.OOE-13 1.50E-13
5/6/1996 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 B.OOE-13 2.25E-13 p.OOE-13 1.50E-13
iB/5/1996 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13
).1/6/1996 9.00E-14 2.25E-14 Z.OOE-14 s.OOE-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13
2/6/1997 9.00E-14 2.25E-14 l.OOE-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E·13
!5/5/1997 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E·13 2.25E-13 6.00E-13 1.50E-13
8/:rl/1!397 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13
1/5/1998 9.00E-14 2.25E-14 2.00E·14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13
4/28/1998 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.SOE-13
7/31/1998 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6,00E-13 1.50E-13
9}28/1998 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13
12/28}1998 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.50E-13
3/29/1999 9.00E-14 2.25E-14 2.00E-14 5.00E-15 9.00E-13 2.25E-13 6.00E-13 1.SOE-13
7/3/1999 9.00E-14 2.25E-14 2.00E-14 S.OOE-15 9.00E-13 2.25E-13 6.00E-13 l.SOE-13
9/27/1999 3.03E-15 9,00E-14 2.25E-14 1.37E-15 2.00E-14 5.00E-15 8.72E-16 9.00E-13 2.25E-13 7.55E-15 6.00E-13 1.50E-13
12/28/1999 5.01E-15 9,00E-14 2.25E-14 2,89E-15 2.00E-14 5.00E-15 1.31E-15 g.OOE-13 2.25E-13 8.10E-15 5.00E-13 l.SOE-13
3/30/2000 7.46E-16 9.00E-14 2.25E-14 5.25E-16 2.00E-14 S.OOE-15 3.00E-16 9.00E-13 2.25E-13 7.83E-15 6.00E-13 l.SOE-13
6/26/2000 5.40E-16 9.00E-14 2.2SE-14 3.53E-16 2.00E·14 S.OOE-15 6.11E-16 9.00E-13 2.25E-13 4.83E-15 6.00E-13 l.SOE-13
9/25/2000 3.75E-16 9.00E-14 2.25E-14 2.23E-16 2.00E-14 5.00E-15 1.91E-16 9.00E-13 2.25E-13 6.41E-15 G,OOE-13 l.SOE-13
12/26/2000 5.21E-16 9.00E-14 2.2SE-14 3.39E-16 2.00E-14 5.00E-15 3.28E-17 9.00E-13 2.25E-13 B.57E-15 6.00E-13 1.50E-13
3/26/2001 1.42E-16 9.00E-14 2.25E-14 l.OOE-16 2.00E·14 5.00E-15 l.OOE-16 9,00E-13 2.25E-13 6.15E-15 6.00E-13 1.50E-13
7/2/2001 1.81E-16 9.00E-14 2.25E-14 1.66E-16 2.00E·14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 6.95E-15 6.00E-13 1.50E-13
9/24/2001 3.08E·16 9.00E-14 2.25E-14 1.01E-16 2.00E-14 5,00E-15 1.77E-16 9 OOE-13 2.25E-13 8.59E-15 G.OOE-13 1.50E-13
12/31/2001 3,31E-16 9.00E-14 2.25E-14 L25E-16 2.00E-14 5.00E-15 1.09E-16 9.00E-13 2.25E-13 3.14E-15 6 OOE-13 1.50E-13
4/1/2002 4.77E-16 9.00E-14 2.25E-14 2.94E-16 2.00E-14 5.00E-15 1.96E-16 9.00E-13 2.25E-13 8.61E-15 6.00E-13 1.50E-13
7/1/2002 3.68E-16 9.00E-14 2.25E-14 4.41E-16 2.00E-14 5.00E-15 1.76E-16 9.00E-13 2.25E-13 8.20E-15 6.00E-13 1.50E-13
9/30/2002 3.67E-16 9.00E-14 2.25E-14 5.60E-16 2.00E-14 5.00E-15 1.80E-16 9.00E-13 2.25E-13 5.55E-15 6.00E-13 1.50E-13
12/30/2002 l.OOE-16 9.00E-14 2.25E-14 3.43E-16 2.00E-14 5,00E-15 1.67E-16 9.00E-13 2,25E-13 135E-14 6.00E-13 1,50E-13
3/31/2003 1.98E-16 9.00E-14 2.25E-14 1.68E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 7.77E-15 6.00E-13 l.SOE-13
6/30/2003 1.18E-16 9.00E-14 2.25E-14 1.15E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 5.92E-15 6.00E-13 1.50E-13
9/29}2003 l.OOE-16 9.00E-14 2.25E-14 1,00E-16 2.00E-14 5.00E-15 l.OOE-16 9.00E-13 2.25E-13 8.30E-15 6.00E-13 1.50E-13
12/29/2003 l.OOE-16 9.00E-14 2.25E-14 1.36E-16 2.00E-14 5.00E-15 l.OOE-16 9,00E-13 2,25E-13 6,66E-15 G.OOE-13 1.50E-13
3/29/2004 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 8.17E-15 6.00E-13 1,50E-13
6/27/2004 l.OOE-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 3.55E-15 6.00E-13 1.50E-13
9/27/2004 1.00E-16 9.00E-14 2.25E-14 1.38E-16 2.00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.22E-14 6.00E-13 1.50E-13
12/27/2004 1.05E-16 9.00E-14 2.25E-14 1.72E-16 2.00E-14 .S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 1.52E-14 6.00E-13 1.50E-13
3/28/2005 l.OOE-16 9.00E-14 2.25E-14 l.OOE-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 9.34E-15 6.00E-13 1.50E-13
6m!'2oos 1.28E-16 9,00E-14 2.25E-14 1.01E-16 2,00E-14 S.OOE-15 l.OOE-16 9.00E-13 2.25E-13 9.85E-15 6.00E-13 1.50E-13
9/26/2005 1,98E-16 9.00E-14 2.25E-14 5.98E-16 2.00E-14 S.OOE-15 3.55E-16 9.00E-13 2.25E-13 1.71E-14 6.00E-13 1.SOE-13
1/3/2006 7.67E-16 9.00E-14 2.25E-14 2.88E-16 2.00E-14 S.OOE-15 3.60E-15 9.00E-13 2.25E-13 4.85E-14 6.00E-13 1.50E-13
4/3}2006 2.92E-16 9.00E-14 2.25E-14 .Z,OOE-16 2.00E-14 S.OOE-15 1.00E-16 9.00E-13 2.25E-13 l.llE-14 6.00E-13 1.50E-13
7/3/2006 3.25E-16 9.00E-14 2.25E-14 2.36E-16 2.00E-14 S.OOE-15 1.08E-16 9.00E-13 2,25E-13 l.lOE-14 6.00E-13 1.50E-13
10/2/2006 5.03E-16 9.00E-14 2.25E-14 1.49E-16 Z.OOE-14 5,00E-15 1.19E-16 9.00E-13 2,25E-13 2.13E-15 6.00E-13 1.SOE-13
1/1/2007 8.31E-16 9.00E-14 2.25E-14 2.49E-16 2.00E-14 5.00E-15 1,00E-16 9.00E-13 2.2SE-13 1.70E-14 6,00E-13 1.50E-13
4/2/2007 5.36E-16 g.OOE-14 2.25E-14 3.15E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.43E-14 6.00E-13 l.SOE-13
7/2/2007 1.08E-15 9.00E-14 2.25E-14 2.18E-16 2.00E-14 5.00E-15 1.54E-16 9.00E-13 2.25E-13 2,04E-14 6.00E-13 1.50E-13
9/30/2007 3.92E·16 9.00E-14 2.25E-14 1.02E-16 2.00E-14 5.00E-15 l.OOE-16 9 OOE-13 2.25E-13 6.38E-15 6.00E-13 l.SOE-13
12/31/2007 2.92E-15 9.00E-14 2.25E-14 1.55E-15 2.00E-14 S,OOE-15 3 16E-16 9.00E-13 2.25E-13 9.19E-15 6 OOE-13 1.50E-13
3/31/2008 4.34E-16 9.00E-14 2,25E-14 3.51E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 5.99E-15 6.00E-13 1.50E-13
6/3102008 1.88E-15 9.00E-14 2,25E-14 9.00E-16 2.00E-14 S.OOE-15 4.04E-16 ll.OOE-13 2.25E-13 7.41E-15 6.00E-13 1.50E-13 -----------
bate Effluent Concentration Limit= 9E-14 uCi/ml I!HV-6U Effluent Concentration Limit = ZE-14 uCi/ml BHV-6T Effluent Concentration Limit = 9E-13 uCi/ml BHV-6R Effluent Concentration Limit= 6E-13 uCi/ml BHV-6PB
ALARAGoal = 2.25E-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = Z.25E-13 uCi/ml ALARA Goal= l.SE-13 uCi/ml
Pre 1994 MPC Limit= SE-12 uCi/ml Pre 1994 MPC_llmtt= SE-14 uCi/ml Pre 1994 MPC Limit = ZE-lZ uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml
Pre 1994 ALARA GOAL = l .Z5E-1Z uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL= 1E-1Z uCi/ml
Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA
9/30/2008 4.82E-15 9.00E-14 ~.25E-14 2.10E-15 2.00E-14 5.00E-15 1.27E-15 9,00E-13 2,25E-13 1.00E-14 6.00E-13 1.50E-13
12/31/2008 4.80E-15 9.00E-14 2.25E-14 l.?OE-15 2.00E-14 5.00E-15 1.25E-15 9.00E-13 2.25E-13 1.49E-14 6.00E-13 1.50E-13
3/15/2009 2.77E-15 ~.OOE-14 2.25E-14 1.01E-15 2.00E-14 5,00E-15 7.82E-16 9.00E-13 2.25E-13 6.46E-15 6.00E-13 1.50E-13
6/15/2009 1.41E-16 9.00E-14 2.25E-14 2.67E-16 2.00E-14 5.00E-15 1.81E-16 9.00E-13 2.25E-13 5.76E-15 6.00E-13 1.50E-13
9/15/2009 4.87E-15 9.00E-14 2.25E-14 /1.32E-16 2.00E-14 5.00E-15 2.23E-16 9.00E-13 2.25E-13 8.98E-15 6.00E-13 1.50E-13
12/15/2009 9.24E-15 9.00E-14 2.25E-14 2,26E-16 2.00E-14 5.00E-15 1.15E-16 9.00E-13 2.25E-13 6.44E-15 6,00E-13 1.50E-13
3/31/2010 9.63E-15 9.00E-14 2.25E-14 1.82E-16 2.00E-14 5.00E-15 :Z.06E-16 9.00E-13 2.25E-13 1.37E-14 6,00E-13 1.50E-13
6/30/2010 3.62E-15 9.00E-14 2,25E-14 3.94E-16 2.00E-14 5.00E-15 4.89E-16 9,00E-13 2.25E-13 4.30E-15 6.00E-13 1.50E-13
9/30/2010 5.42E-15 ·, 9.00E-14 2.25E-14 1.08E-15 2.00E-14 5,00E-15 5.68E-16 9.00E-13 2.25E-13 3.98E-15 6.00E-13 1,50E-13
12/31/2010 1.24E-14 9.00E-14 2.25E-14 1.21E-15 2.00E-14 S.OOE-15 l.OOE-15 9.00E-13 2.25E-13 1.53E-14 6.00E-13 1.SOE-13
4/4/2011 2.70E-15 9.00E-14 2.25E-14 4.62E-16 2.00E-14 S.OOE-15 6.51E-16 S.OOE-13 2.25E-13 1.29E-14 -6.00E-13 1.50E-13
7/4/2011 . 3.01E-15 9.00E-14 2.25E-14 7,07E-16 2.00E-14 S.OOE-15 5.75E-16 9.00E-13 2.25E-13 7.97E-15 6.00E-13 1.50E-13
10/3/2011 2.05E-15 9.00E-14 2.25E-14 6.12E-16 2.00E-14 ,S.OOE-15 1.88E-16 9,00E-13 2.25E-13 9.93E-15 6.00E-13 1.50E-13
1/3/2012 3.14E-15 9.00E-14 2.25E-14 1.09E-15 2.00E-14 S,OOE-15 7.65E-16 9,00E-13 2.25E-13 1.89E-14 G.OOE-13 1.50E-13
4/3/2012 4.41E-15 9.00E-14 2.2SE-14 1.82E-15 2.00E-14 S.OOE-15 4.00E-16 9.00E-13 2.25E-13 1.50E-14 6.00E-13 1.50E-13
7/2/2012 6.42E-15 9.00E-14 2.25E-14 2.25E-15 2.00E-14 'S.OOE-15 5.11E-16 9.00E-13 2.25E-13 9.54E-15 6.00E-13 1.SOE-13
10/1/2012 6.63E-15 9.00E-14 2.25E-14 1.31E-15 2.00E-14 S.OOE-15 1.22E-15 9.00E-13 2,25E-13 1.34E-14 6.00E-13 1.50E-13
12/31/2012 3.83E-15 9.00E-14 2.25E-14 1.18E-15 2.00E-14 S.OOE-15 9.30E-16 9.00E-13 2.25E-13 1.60E-14 6.00E-13 1.50E-13
3/25/2013 4.52E-15 9.00E-14 2.25E-14 7.93E-16 2.00E-14 S.OOE-15 4,91E-16 g.OOE-13 2.25E-13 1.70E-14 6.00E-13 1.50E-13
7/2/2013 5.91E-15 9.00E-14 2.25E-14 6.74E-16 2.00E-14 S.OOE-15 7.85E-16 9.00E-13 _ 2.2SE·131~18E:1s 6.00E-13 1.50E-13
---
U) c 0
'+=i ctl """ -c G)
(.) c 0 0
G) ,
(.)
:::l c
0 ,
ctl a:
co > ::I: m
N .-I w
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~
-I
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t.
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li
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1111
t::=o jP
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I
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-
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--
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~ -
, . .
----
-----
-----
-
----
1-
co
t.U .-
~ ~Oc/8/0~
800c/08/6
900c/9G/6
0 .-N I -a ro Q)
...J
cOOc/08/6 +
c.o N N
E:
666 ~/LG/6:6
ro a:
+
966~/9/8 g
N
E:
:J ·;::
0 ..c
866 ~/0~/8+
~ :J
066 ~/8~/8~
E :J c ~ ::::>
L86~/6/6 +
1786 ~/ ~/0 ~
~86 ~/8G/6
1.00E-11
1.00E-12
1.00E-13
Q)
(ij u ~ .OOE-14
0> 0 _J -
1.00E-15
1.00E-16
1.00E-17
-
-
.....
CX)
0) ..... ro ~ 0)
Effluent Concentration Limit= 9E-14 uCi/ml
ALARA Goal= 2.25E-14 uCi/ml
Pre 1994 MPC Limit= 5E-12uCi/ml
Pre 1994 ALARA Goal= 1.25E-12 uCilml
' '
""'" CX)
0) ..... ..._ ..... ..._
0
' . .
t--oo
0) ..... 05 ..._
0)
. ' 0 0)
0)
~ ..... ro
' ' . .
C')
0)
0)
25 ..... ro
It I .
BHV-6 Uranium-Natural Concentrations (uCi/ml)
' (!)
0)
0) ..... ..._
LO ro
t t j
..J.c
J I I t
0)
0)
0) ..... ..._
1'-~
'
"" •\ ~~
1
Jl'
' '.
\
\A.
.
0 0 ~ ~
'.
.... r
l4 1 ....
.J
f i i
0 0 ~ ~
..
t I I i
" I \
I
0 0 ~ ~
-
.
t
-
1/ •
'
. \.:. ....... ....
"V
I t¥ I_ I
..... 0 ~ 0
-
"' r:::: 0
~ ca "--r:::: Q)
C)
r:::: 0 0
0 C")
N I E
::::J 'i: 0 .r:::: I-
CO :> :I: m
.... w
0 0 ....
C\1 .... I w 0 C! ....
C') .... I w 0 C! ....
• ~
'
~~~
~r-.
-""'
"<:t ll) .... .... I I w w 0 0 0 C! (are~s oo1)
~ ~Oc/8/0~
l .... ~ F:~ •
800G/08/6
I
~~~ ~
~ ~ . .
SOOc/9G/6
:~ -
j -.
.. -.
cOOc/08/6
...... ~ ~ -
~.-: fi .
666 ~/LG/6 -
-. . 966 ~/S/8 . . -. ---. . .
-866 ~/0~/8 . ---.
-066 ~/8 ~/8 -. -
L86~/6/6
-.
' . -'1786 ~/~/0~ . . --
-. --~86 ~/8G/6
CD I'-.... I w w 0 0 C! C! ....
Cl) c 0 -~ -c Cl) u c 0 0
(0
N N I
E ::I
"'C cu a:
(0 :> :I: m
..-..-I L.U
0 ~
,_.,. ~o-1-
C\1 ..-I L.U 0 ~ ..-
I •
a:
...
(t) '<;!" l() ..-..-I I w L.U L.U 0 0 0 ~ 0 ~ ..-(areos oo1)
• -
~ .
~t::o· --~ ~oc/8/0 ~ -
I
~~-h .
~ .
~ -
800c/08/6
~~~ ==-~ -900c/9c/6
.
--~ .
-
cOOc/08/6
-.
F= . . 666~/LG/6
966 ~/9/8
.
-
-866 ~/0~/8
-
-066 ~/8 ~/8
-
-L86 ~/6/6 -----------'1786 ~/~/0~ --------~86 ~/8c/6
co ,.....
..-..-
I I L.U L.U
0 0 ~ ~ ..-..-
1.00E-11
1.00E-12
1.00E-13
Q)
Cii ~ .OOE-14
0> 0 __J -
1.00E-15
1.00E-16
1.00E-17
-
Effluent Concentration Limit= 6E-13 uCi/ml
ALARA Goal= 1.5E-13 uCi/ml
Pre 1994 MPC Limit= 4E-12uCilml
Pre 1994 ALARA Goal= 1 E-12 uCi/ml
I t r I t ' '.' ' ' ~ .... -.;t co co Ol Ol .... .... -.. -.. co .... ~ -.. 0 Ol
,..._
co Ol .... -.. Ol -.. Ol
0 Ol Ol ....
Ct5 ....
Ci5
• I I I I
C')
Ol Ol
~ ....
Ci5
BHV-6 Lead-21 0 Concentrations (uCi/ml)
I I o o 0 0 I \ L I I .
<.0 Ol Ol .... -.. LO Ci5
Ol Ol Ol .... ;:::
~
...
~
'
-II
I
~ ~!
1"1 •
' ' t ~ I ' I I I t <
C\1 0 0 2l ~
0 0 ~ <.0 ~
l. M
-
' '
Jt
' 11
0 0 2l ~
1 r.tM .
-&.I
It I I I I II J I
.... 0 ~ 0
ATTACHMENT C
BHV AIR SAMPLING LABORATORY RESULTS AND QNQC
Helena, MT B77-472-D711 • Bllllnp, MT 801-731-4419 • Casper, WY 888-235-0515
Glllstta, WY 118-111-7175 • Rapid City, SD 118-172-m5 • CollogeStatlon. IX 881-680-2218
May 22, 2013
Energy Fuels Resources (USA) Inc
225 Union Blvd Ste 600
Lakewood, CO 80228-1826
Workorder No.: C13040210
Project Name: 1st Quarter Air 2013
ANALYTICAL SUMMARY REPORT
Energy Laboratories, Inc. Casper WY received the following 6 samples for Energy Fuels Resources (USA) Inc on 4/4/2013 for
analysis.
Sample ID Client Sample ID Collect Date Receive Date Matrix Test
C13040210-001 BHV-1 03/25/13 00:00 04/04/13 Filter Composite of two or more samples
Metals, Total
C13040210-002 BHV-2
C13040210-003 BHV-4
C 1304021 0-004 BHV -5
C13040210-005 BHV-6
C13040210-006 Blank
03/25/13 00:00 04/04/13
03/25/13 00:00 04/04/13
03/25/13 00:00 04/04/13
03/25/13 00:00 04/04/13
03/25/13 00:00 04/04/13
Filter
Filter
Filter
Filter
Filter
Digestion, Total Metals
Lead 210
Radium 226
Thorium, Isotopic
Same As Above
Same As Above
Same As Above
Same As Above
Same As Above
The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were
performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted.
Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601,
unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical
Report, the QNQC Summary Report, or the Case Narrative.
If you have any questions regarding these test results, please call.
Digitally signed by
Steve Carlston Report Approved By: ;/ ./""? ~~-----~'-b. r ie-i,r ~
)'V l~t;;rim Branch Manager
Date: 2013.05.22 18:20:03 -06:00
Page 1 of22
Halana, MT 877·472..0711 • Blllln&s. MT 800-735·4489 • Casper, WY 881-235-0515
Gllfalte WY 81S..I86·71l5 • Ra ld C SO 888-172-1225 • Colle c Statton TX 888-&90-2218
CLIENT: Energy Fuels Resources (USA) Inc
Project: 1st Quarter Air 2013
Sample Delivery Group: C1304021 0
Report Date: 05/22/13
CASE NARRATIVE
Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Ad., College
Station, TX, EPA Number TX01520.
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are
hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has
begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated~
ATAAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for
seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria
for PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize
its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b-Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. - Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r-Energy Laboratories, Inc. -Rapid City, SD
eli-cs -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641 , Radiochemical E871 017; California: 02118CA;
Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify Ell's certification coverage by visiting www.energylab.com
Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com .
Page 2 of22
www.energyfab.com
..,._~SIIcl IISZ
Helena, MT 877-472-0711 • Billings, MTIOD-735-4481 • Casper, WY 888-235-0515
Gillette, WY 88&-688-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-&90-2218
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: May 22, 2013
PROJECT: 1st Quarter Air 2013
SAMPLE ID: BHV-1
Quarter/Date Sampled Concentration Radionuclide Air Volume 11CilmL
C13040210-001 nalu 9.91E-16
First Quarter 2013 2JoTh 1.86E-16
Air Volume in mLs 226Ra 2.04E-16
1.36E+ll 210Pb 1.82E-14
+LLD's are from Reg. Guide 4.14
Counting
Precision
J.!CilmL
N/A
SE-17
lE-17
2E-16
*Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDCfJCi/mL
N/A
2E-17
4E-18
SE-17
L.L.D.+ Effluent Cone.* %Effluent
fJCi/mL 11CilmL Concentration
lE-16 9E-14 1.10E+00
1E-16 3E-14 6.21E-01
1E-16 9E-13 2.27E-02
2E-15 6E-13 3.03E+00
Page 3 of22
EI\ERGY
',.. ••• ; f"'
Helena, MT 871·472-G711 • Billings, MT 800·735-4489 • Casper, WY 881·235·0515
Gillette, WY 811-118·7175 • Rapid City, SD 888-172·1225 • College Station, TX 881·69D·2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 05/22/13
Collection Date: 03/25/13
DateReceived: 04/04/13
Matrix: Filter
Project: 1st Quarter Air 2013
Lab ID: C1304021 0-001
Client Sample ID BHV-1
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 21 0 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
0.199 mglfilter
135 pCiiFilter
2480 pCi/Filter
24 pCiiFilter
7.5 pCiiFilter
27.8 pCiiFilter
2.0 pCi/Filter
0.6 pCiiFilter
25 pCiiFilter
6.5 pCiiFilter
3.0 pCiiFilter
MDC-Minimum detectable concentration
MCU
Qualifiers RL QCL Method Analysis Date I By
0.0003 SW6020 04111113 22:30 I elm
0.2 SW6020 04111/13 22:30 I elm
E909.0 04118113 o 1 :39 I eli-cs
E909.0 04118113 01 :39 I eli-cs
E909.0 04118113 o 1 :39 I eli-cs
E903.0 04117113 13:561 trs
E903.0 04117/1313:561trs
E903.0 04117113 13:561 trs
E908.0 0411211317:151dmf
E908.0 04112/13 17:15 I dmf
E908.0 04112113 17:15 I dmf
MCL-Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 4 of22
www.energylab.com
AIMI1fla/ ~ Sllct JISZ
Helena, r.rr 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-&86-7115 • Rapid City, SO 888-&72-1225 • College Station,lX 888-690·2218
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: May 22, 2013
PROJECT: 1st Quarter Air 2013
SAMPLE ID: BHV-2
Quarter/Date Sampled Concentration Radionuclide Air Volume J1CilmL
c 1304021 0-002 nalu 3.38E-16
First Quarter 2013 23UTh 3.94E-17
Air Volume in mLs 226Ra 8.32E-17
1.36E+ll 210Pb 1.42E-14
+LLD's are from Reg. Guide 4.14
Counting
Precision
J.1Ci/mL
N/A
lE-17
9E-18
2E-16
*Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDCJ.1Ci/mL
N/A
9E-18
4E-18
SE-17
L.L.o.• Effluent Cone.* %Effluent
J1CilmL J1Ci/mL Concentration
1E-16 9E-14 3.75E-01
1E-16 3E-14 1.31E-01
1E-16 9E-13 9.25E-03
2E-15 6E-13 2.37E+00
Page 5 of22
EN:RGY
, H \I ~ ~~
Halana, MT 811-472-0711 • Billings, MT BOD-735-4489 • Casper, WY 881-235-0515
Gillatta, WY 81&-188-7175 • Rapid City, SD 888-172-1225 • Collega Stltion, TX 888-690-2218
LABORATORY ANAL VTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc Report Date: 05/22/13
Collection Date: 03/25/13
DateReceived: 04/04/13
Matrix: Filter
Project: 1st Quarter Air 2013
Lab ID: c 1304021 0-002
Client Sample ID BHV-2
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIO NUCLIDES
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±}
Radium 226 MDC
Thorium 230
Thorium 230 precision (±}
Thorium 230 MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL-Quality control limit.
Result Units
0.0679 mglfilter
46.0 pCiiFilter
1940 pCiiFilter
21 pCi!Filter
7.5 pCiiFilter
11.3 pCiiFilter
1.3 pCiiFilter
0.6 pCiiFilter
5.4 pCiiFilter
1.7 pCiiFilter
1.2 pCiiFilter
MDC -Minimum detectable concentration
MCU
Qualifiers RL QCL Method Analysis Date I By
0.0003 SW6020 04111113 22:36 I elm
0.2 SW6020 04111113 22:36 I elm
E909.0 04118113 01 :39 I eli-cs
E909.0 04118113 01 :39 I eli-cs
E909.0 04118113 01 :391 eli-cs
E903.0 04117113 13:56/trs
E903.0 04117113 13:561 Irs
E903.0 04117113 13:56 I Irs
E908.0 04112113 17:151 dmf
E908.0 04112/13 17:15 I dmf
E908.0 04112113 17:15 I dmf
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 6 of 22
www.energylab.com
AM/ffkallmii~¢.SI-IISZ
Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, WY 881-235-0515
Gillette, WY 8&&-&81-7115 • Rapid City, SD 818-172-1225 • College Station, 1X 881-&90-2218
ffiGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: May 22, 2013
PROJECT: 1st Quarter Air 2013
SAMPLE ID: BHV -4
Quarter/Date Sampled Concentration Counting
Air Volume Radionuclide J!CilmL
C13040210-003 ""U 3.04E-15
First Quarter 2013 230Th 4.99E-16
Air Volume in mLs 226Ra 2.79E-16
1.35E+ll 210Pb 2.13E-14
+LLD's are from Reg. Guide 4.14
*Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
Precision
J!Ci/mL
N/A
9E-17
2E-17
2E-16
MDCJ!Ci/mL
N/A
2E-17
4E-18
SE-17
-_
L.L.D.+ Effluent Cone.* %Effluent
11CilmL J!CilmL Concentration
IE-16 9E-14 3.38E+00
1E-16 3E-14 1.66E+OO
IE-16 9E-13 3.10E-02
2E-15 6E-13 3.54E+00
Page 7 of22
EN:RGY
' _ 1 • I'~ ltJ
www.energylab.com
A-'1fiai~SIIa lfiZ
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Caspar, WY 811-235-0515
Gillette, WY 11&-186-7175 • Rapid City, SD 81&-172-1225 • College Station, TX 881-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 1st Quarter Air 2013
Lab ID: c 1304021 0-003
Client Sample ID BHV-4
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
0.608 mglfilter
411 pCiiFilter
2880 pCi/Filter
26 pCiiFilter
7.3 pCiiFilter
37.8 pCiiFilter
2.2 pCiiFilter
0.5 pCiiFilter
68 pCiiFilter
13 pCiiFilter
2.5 pCiiFilter
MDC-Minimum detectable concentration
Qualifiers
MCU
RL QCL
0.0003
0.2
Report Date: 05/22/13
Collection Date: 03/25/13
DateReceived: 04/04/13
Matrix: Filter
Method Analysis Date I By
SW6020 04111113 22:39 I elm
SW6020 04111113 22:39 I elm
E909.0 04118113 01 :39 I eli-cs
E909.0 04118113 01 :39 I eli-cs
E909.0 04118113 01 :39 I eli-cs
E903.0 04117113 13:56 I trs
E903.0 04117113 13:56 I trs
E903.0 04117113 13:56 I trs
E908.0 04112113 17:15 I dmf
E908.0 04112113 17:15 I dmf
E908.0 0411211317:151dmf
MCL-Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 8 of22
EI\ERGY
.. '.. •JI .J
www.energylab.com
Allfl1lk:tl Ei.ullllli:f .. last
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: May 22,2013
PROJECT: 1st Quarter Air 2013
SAMPLE ID: BHV-5
Quarter/Date Sampled Concentration Radionuclide Air Volume J.!CilmL
C13040210-004 nalu 6.66E-15
First Quarter 2 0 13 230Th 1.48E-15
Air Volume in mLs 226Ra 1.12E-15
1.35E+ll 210Pb 1.80E-14
+LLD's are from Reg. Guide 4.14
Counting
Precision
11CilmL
N/A
3E-16
3E-17
2E-16
*Effluent Concentration from the NEW I 0 CFR Part 20 -Appendix B -Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDCJJCilmL
N/A
4E-17
4E-18
SE-17
L.L.D.+ Effluent Cone.* %Effluent
J.!CilmL 11CilmL Concentration
IE-16 9E-14 7.40E+00
IE-16 3E-14 4.95E+00
IE-16 9E-13 1.24E-01
2E-15 6E-13 3.00E+00
Page 9 of22
www.energylab.com EN:RGY
"" · .,..l • • I • r 'J I '~ Al/llfflal ~ SiJu rnz
Helena, MT 877·472-G711 • Billings, MT 800·735-4489 • Casper, WY 881-235·0515
Gillette, WY 81&-18&·7175 • Rapid City, SD 888-172-1225 • College Station, TX 881·690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 1st Quarter Air 2013
Lab ID: C1304021 0-004
Client Sample ID BHV-5
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 210 precision(±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
1.33 mglfilter
901 pCiiFilter
2430 pCiiFilter
24 pCiiFilter
7.4 pCiiFilter
151 pCiiFilter
4.2 pCiiFilter
0.5 pCiiFilter
201 pCiiFilter
35 pCiiFilter
5.7 pCi!Filter
MDC -Minimum detectable concentration
Qualifiers
MCLJ
RL QCL
0.0003
0,2
Report Date: 05/22/13
Collection Date: 03/25/13
DateReceived: 04/04/13
Matrix: Filter
Method Analysis Date I By
SW6020 04111113 23:041 elm
SW6020 04111113 23:041 elm
E909.0 04118113 o 1 :39 I eli-cs
E909.0 04118113 01 :39 I eli-cs
E909.0 04118113 o 1 :39 I eli-cs
E903.0 04117113 13:561 trs
E903.0 04117113 13:561 trs
E903.0 04117113 13:561 trs
E908.0 0411211317:151dmf
E908.0 04112113 17:151 dmf
E908.0 04112113 17:151 dmf
MCL -Maximum contaminant level.
ND-Not detected at the reporting limit.
Page 10 of 22
www.energylab.com
Allf1lka/ Eluli«!U smr. IW
Helena, MT 877-472-0711 • Billings, MT 1100-135-4489 • Casper, WY 888-235-0515
Gillette, WY 8&6-&8&-7175 • Rapid City, SO 888-612-1225 • College Station, TX 8811-&90-2218
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: May 22, 2013
PROJECT: 1st Quarter Air 2013
SAMPLE ID: BHV-6
Quarter/Date Sampled Concentration Radionuclide Air Volume ,..cilmL
c 13040210-005 nalu 4.52E-15
First Quarter 2013 230Th 7.93E-16
Air Volume in mLs 226Ra 4.91E-16
1.35E+ll 210J>b 1.70E-14
+LLD's are from Reg. Guide 4.14
Counting
Precision
,..cilmL
N/A
2E-16
2E-17
2E-16
*Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
Moc,..cilmL
N/A
4E-17
4E-18
6E-17
L.L.D.+ Effluent Cone.* %Effluent
,..cilmL ,..cilmL Concentration
IE-16 9E-14 5.02E+00
IE-16 3E-14 2.64E+00
IE-16 9E-13 5.46E-02
2E-15 6E-13 2.83E+00
Page 11 of 22
EN:RGY
l\·· -'1~ '1• .. 1·1 -
www.energylab.com
W/flfai~Sinw IIU
Helena, MT B71·412-Q711 • Billings, MT 808-735-4489 • Casper, WY 881·235-8515
Gillette, WY 818-18&·7175 • Rapid City, SD 818-172-1225 • College Station, TX 881-&90-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 1st Quarter Air 2013
Lab ID: C1304021 0-005
Client Sample ID BHV-6
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 21 0 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
0.902 mglfilter
611 pCi/Filter
2290 pCiiFilter
23 pCiiFilter
7.4 pCiiFilter
66.4 pCiiFilter
2.9 pCiiFilter
0.5 pCiiFilter
107 pCiiFilter
21 pCiiFilter
5.1 pCiiFilter
MDC -Minimum detectable concentration
Qualifiers
MCU
RL QCL
0.0003
0.2
Report Date: 05/22/13
Collection Date: 03/25/13
DateReceived: 04/04/13
Matrix: Filter
Method Analysis Date I By
SW6020 04111113 23:07 I elm
SW6020 04111113 23:07 I elm
E909.0 04118113 01:39 I eli-cs
E909.0 04118113 01 :39 I eli-cs
E909.0 04118113 01 :39 I eli-cs
E903.0 04117113 13:56 /Irs
E903.0 04117113 13:56 /Irs
E903.0 04117113 13:56 I trs
E908.0 04112113 17:15 I dmf
E908.0 0411211317:151dmf
E908.0 0411211317:151dmf
MCL -Maximum contaminant level.
NO-Not detected at the reporting limit.
Page 12 of 22
EN:RGY ......
www.enlifgylab.com
AMiytlal ~ Slra 1151
Helena, MT 871-472-0711 • Billings, MT 100-735-4489 • Casper, WY IBB-235-0515
Gillette, WY 811-&BI-7175 • Rapid City, SD BIB-&72-1225 • College Station, lX IBB-&90-2211
IDGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: May 22, 2013
PROJECT: 1st Quarter Air 2013
SAMPLE ID: Blank
Quarter/Date Sampled Concentration Counting
Radionuclide Precision Air Volume !JCilmL !JCilmL
c 13040210-006 ""U 9.60E-18 N/A
First Quarter 2013 2>oTh 3.27E-18 3E-18
Air Volume in I11L.s 226Ra 3.89E-18 3E-18
1.36E+I I 210Pb -4.09E-17 3E-17
Note: This sample uses 136,000,000 L of air volume for comparison purposes.
+LLD's are from Reg. Guide 4.14
*Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-21 0
MDC!JCilmL
N/A
6E-18
4E-18
SE-17
L.L.D.+ Effluent Cone.* %Effluent
!!CilmL !JCilmL Concentration
lE-16 9E-14 l.O?E-02
IE-16 3E-14 1.09E-02
IE-16 9E-13 4.32E-04
2E-15 6E-13 -6.82E-03
Page 13 of 22
ww.energyleb.com EN:RGY
" . ,t ~. • , 1. r n, ~ Alf'l1llol £ll:8llillu ss-11!1
Helene, MT 877-472-1711 • Billings, MT 800-735-4489 • Casper, WY 881-235-0515
Gillette, WY 818-181-7175 • Rapid City, SD 818-i12-1225 • Collage Station, TX 811-&10-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 1st Quarter Air 2013
Lab ID: C1304021 0-006
Client Sample ID Blank
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 210 precision(±)
Lead 210 MDC
Radium226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
0.0019 mglfilter
1.3 pCiiFilter
-6 pCi/Filter
4.3 pCi!Filter
7.4 pCiiFilter
0.5 pCiiFilter
0.4 pCiiFilter
0.5 pCi!Filter
0.44 pCiiFilter
0.46 pCiiFilter
0.82 pCiiFilter
MDC -Minimum detectable concentration
Qualifiers
u
u
RL
0.0003
0.2
MCLI
Report Date: 05/22/13
Collection Date: 03/25/13
DateReceived: 04/04/13
Matrix: Filter
QCL Method Analysis Date I By
SW6020
SW6020
E909.0
E909.0
E909.0
E903.0
E903.0
E903.0
E908.0
E908.0
E908.0
04111 113 23:10 I elm
04111113 23:10 I elm
04118113 01 :391 eli-cs
04118113 01 :391 eli-cs
04118113 01 :39 1 eli-cs
04/17113 16:56/trs
04/17113 16:56 I Irs
04117/13 16:56/trs
04112/13 17:151 dmf
04112113 17:15/ dmf
04112113 17:15/ dmf
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Page 14 of 22
EI\ERGY
•, I 11.-L('•-Il •
www.energylab.com
AM(Jtbi~Sita rm Helena, MT 877-472-41711 • Billings, MT 808-735-4489 • Casper, WY 811-235-1515
Gillatta, WY 816-181-7175 • Rapid City, SD 118-172-1225 • College Station, TX 881-&10-2211
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 1st Quarter Air 2013
Analyte Count Result Units
Method: E200.8
Sample ID: MB-37074 2 Method Blank
Uranium ND mg/L
Uranium, Activity ND pCi/L
Sample ID: LCS2-37074 Laboratory Control Sample
Uranium 0.102 mg/L
Sample ID: C1304021 0-003AMS Sample Matrix Spike
Uranium 0.860 pCi/Filter
Sample ID: C1304021 0-003AM SO Sample Matrix Spike Duplicate
Uranium 0.862 pCi/Filter
Qualifiers:
RL -Analyte reporting limit.
MDC -Minimum detectable concentration
RL %REC
6E-05
0.04
0.00030 102
0.00030 106
0.00030 107
Report Date: 05/22/13
Work Order: C1304021 o
Low Limit High Limit RPD RPDLimit Qual
Batch: 37074
Run: ICPMS2-C_130411A 04/11/13 22:17
Run: ICPMS2-C_130411A 04/11/13 22:20
85 115
Run: ICPMS2-C_130411A 04/11/13 22:55
70 130
Run: ICPMS2-C_130411A 04/11 /13 22:58
70 130 0.2 20
ND -Not detected at the reporting limit.
Page 15 of 22
EN:RGY
•'> ./"""1 .·,I·. I·!
www.energylab.com
Anl/blllullfflu S/11:1 IW
Helena, MT 877-472..0711 • Billings, MT 800·731-4489 • Casper, WY 881·235-0515
Glllatta, W'f 816-188-7115 • Rapid City, SO 816-172-1225 • College Station, 1X 881-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 1st Quarter Air 2013
Analyte
Method: E903.0
Sample ID: C13040162-001 HMS
Radium 226
Sample ID: C13040162-001HMSD
Radium 226
Sample ID: LCS-37074
Radium 226
Sample ID: MB-37074
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Qualifiers:
RL-Analy1e reporting limit.
Count Result Units
Sample Matrix Spike
18 pCi/L
Sample Matrix Spike Duplicate
19 pCi/L
Laboratory Control Sample
20.1 pCi/Filter
3 Method Blank
0.09 pCi/Filter
0.2 pCi/Filter
0.4 pCi/Filter
MDC-Minimum detectable concentration
Report Date: 05/22/13
Work Order: C1304021 0
RL %REC Low Limit High Limit RPD RPDLimit Qual
Run: BERTHOLD 770-2_130411A
101 70 130
Run: BERTHOLD 770-2_130411 A
106 70 130 4.5
Run: BERTHOLD 770-2~ 130411A
94 80 120
Run: BERTHOLD 770-2_130411A
NO -Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Batch: 37074
04/17/13 13:56
04/17/13 13:56
22.3
04/17/1316:56
04/17/13 16:56
u
Page 16 of 22
Er\ERGY
• . I ' ·~I ' .. ~I ,
www.energylab.com
~lbcflllauSiru rm Helena, MT 877-472-8711 • Billings, MT 808·735-4489 • Casper, WY 881-235·8515
Gillatta, WV 11&-188-7175 • Rapid City, SD 818-172-1225 • College Station, TX 881-&90-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 1st Quarter Air 2013
Analyte
Method: E908.0
Sample 10: C13040162-001HMS
Thorium 230
Sample 10: C13040162-001HMSO
Thorium 230
Sample 10: LCS-37074
Thorium 230
Sample 10: MB-37074
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Qualifiers:
RL-Analy1e reporting limit.
Count Result Units
Sample Matrix Spike
19 pCi/L
Sample Matrix Spike Duplicate
16 pCi/L
Laboratory Control Sample
23.2 pCi/Filter
3 Method Blank
0.4 pCi/Filter
0.4 pCi!Filter
0.8 pCi!Filter
MDC-Minimum detectable concentration
Report Date: 05/22/13
Work Order: C13040210
RL %REC Low Limit High Limit RPO RPOLimit Qual
Run: ALPHANALYST_130411A
116 70 130
Run: ALPHANALYST_130411A
99 70 130 16
Run: ALPHANALYST_130411A
99 80 120
Run: ALPHANALYST_130411A
ND -Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Batch: 37074
04/12113 17:15
04/12113 17:15
45.2
04/12113 17:15
04/12113 17:15
u
Page 17 of 22
EN:RGY
~ ~' \ l : :• I . '
www.energylab.com
AMIItfgflluiiiiCWS.. tm Helena, MT 877-472-8711 • Billings, MT 800·735-4489 • Casper, WY 811-235-0515
Gillette, WY 116-188-7175 • Rapid City, SD 816-172-1225 • College Station, lX 881-698-2218
QAJQC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 1st Quarter Air 2013
Analyte
Method: E909.0
Sample ID: LCS-18372
Lead 210
Count Result Units
Laboratory Control Sample
123 pCi/Filter
-This LCS is being reported with PB-18416 as it was prepared at the same time.
Sample ID: MB-18416
Lead 210
Lead 21 0 precision (±)
Lead 210 MDC
Sample ID: T13040058-001AMS
Lead 210
3 Method Blank
-2 pCi/Filter
4 pCi/Filter
7 pCi/Filter
Sample Matrix Spike
2640 pCi/Filter
Report Date: 05/22/13
Work Order: C 1304021 0
RL o/JIEC Low Limit High Limit
Run: SUB-T50472
92 70 130
Run: SUB-T50472
Run: SUB-T50472
70 130
RPD RPDLimit Qual
Batch: T_18416-PB-210-0364
04/18/13 01 :39
04/18/13 01 :39
u
04/18/13 01 :39
-Sample activity for this radionuclide is much larger than the spike activity added. Therefore the matrix spike recovery could not be calculated. The RPD of the MS/MSD
pair are acceptable; this batch is approved.
Sample ID: T13040058-001AMSD
Lead 210
Sample Matrix Spike Duplicate
2480 pCi!Filter
Run: SUB-T50472
70
04/18/13 01 :39
130 6.2 13.7
-Sample activity for this radionuclide is much larger than the spike activity added. Therefore the matrix spike recovery could not be calculated. The RPD of the MS/MSD
pair are acceptable; this batch is approved.
Qualifiers:
RL -Analy1e reporting limit. NO -Not detected at the reporting limit.
MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration
Page 18 of 22
EI\ERGY
•' -; ~ • • I ; "' I
Helena, MT 877-472-11711 • Billings, MT 800-735-4489 • Casper, WY 881-235-0515
Gillette, WY 116-188-7175 • Rapid City, SD 886-172-1225 • College Station, TX 811-690-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 1st Quarter Air 2013
Report Date: 05/22/13
Work Order: C1304021 0
Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimlt Qual
Method: SW6020 Analytical Run: ICPMS2-C_130411A
Sample ID: ICV Initial Calibration Verification Standard 04/11113 10:36
Uranium 0.0500 mg/L 0.00030 100 90 110
Sample 10: ICSA Interference Check Sample A 04/11/13 10:39
Uranium 1.33E-05 mg/L 0.00030
SampleiD: ICSAB Interference Check Sample AB 04/11/13 10:43
Uranium 2.70E-06 mg/L 0.00030
Method: SW6020 Batch: 37074
Sample ID: C1304021 0-001 ADIL Serial Dilution Run: ICPMS2-C_130411A 04/11/13 22:33
Uranium 0.186 mg/filter 0.00030 7.0 20
Sample ID: C1304021 0-003AMS Sample Matrix Spike Run : ICPMS2-C_130411A 04/11/13 22:55
Uranium 0.860 mg/filter 0.00030 106 75 125
SamplelD: C1304021 0·003AM SD Sample Matrix Spike Duplicate Run: ICPMS2-C_130411 A 04/11/13 22:58
Uranium 0.862 mg/filter 0.00030 107 75 125 0.2 20
Sample ID: MB-37074 Method Blank Run: ICPMS2-C_130411A 04/11/13 22:17
Uranium NO mg/filter 6E-05
Sample ID: LCS2-37074 Laboratory Control Sample Run: ICPMS2-C_130411A 04/11 /13 22:20
Uranium 0.102 mg/filter 0.00030 102 85 115
Qualifiers:
RL • Analyte reporting limit. NO -Not detected at the reporting limit.
MDC -Minimum detectable concentration
Page 19 of 22
[11-EI\ERGY
t"LCA~~ t"I'(IN 1 (rroee as mucn mrormat1on as po551Ule,J
Chain of Custody and AnalyJical Request Record Page __L of -i-
Company Name: E Projeot Name, PWS. Perm~Etc. -Sample Origin EPA/State Compliance: ~t,r~'j Fuc-15 \s+-Qu6..r+vA~r ;lol3 state:vl Yes~ NoD
Report Mail Address: 6 &.«~ S. H wy l q I Contact Name: Phone/Fax~ Email: Sampler: (Please Print)
S' t ;A-A \ vT" g&.fSi l / -P.t~ 'il5 671 ::Z.:Z.Z\ SPA.l~ttc:.-u-_!ylV~\r ~ ~ ..:.J u-c:.rf"•tA.. · T,~ ..,...._ ... t.l ... n:Lv
Invoice Address: Invoice Contact & Pho1te: Purchase Order: OuotelBottle Order: '
s~ s~
Special Report/Formats: -s &mi!.W@O® ~@!!!J~ • Contact ELl prior to_ l;.~·~oy: 11 '011
0 ._ RUSH sample submittal I'!(~AA~tl ~_;:::;;;.;,--,.,---'-V _'---t'4
"'0 ., ~ --. for charges and edGier 10{&1: l. m;g~_s 0 ~ R scheduling-See I)... e->~ ca ~ W !::.. Instruction Page ruCf7C 0 OW 0 EDD/EDT(Eiectronic Data) 5~~ ~ > I -o R • T
0 U > o ca = , ' c: Comm ts· eceopt emp POTW/WWTP Format: 0<t:~'~i~ 4: e U en · A (± o
0 State· D LEVEL IV .... m $ c: ·c: 1--ca u.)-C . il C-CU' 0 0 I-c: v( .. "''. 0 Other: 0 NELAC §~i~ () 'C <1: ~ Onlce: N 1
z Ci 4:1 ~0 t ~ t"' <: W 'E S Custody Seal z;) E >1 ~ ~ (' ;:: W t'C On Bottle Y N ~ ~ 1 1 ' (/) ] OnCooler N
1------------...,...-------.-----+-------l ' ~ _<! J cJ5 H Intact y N
SAMPLE IDENTIFICATION Collection Coll~on MATRIX :::l L: tSj D. Signature y N
(Name. Location, Interval, etc.) Date T1me r Match
1 ~ H v _ \ • J 7/1 ~ -3/ ,_~j rJ 12-A ~ )1. >C >< ~
2 R ~ v-~ I .11i\ X )( ~ >' ~
3 rulv-IL4 \ X X >t .~ ~
4 i?H V-5_ ("' 'V' 'f. )( >( J<. ~ ..
s nw.v-i \}7[iJ-)}~/JJ tl-A >' x >< ~. ~-
6 R'lA.A -" > ~ )( X ' X X ~l3dJQiQtO
7 ~
8 ~ 0
9 !
10 ·c:::::
Custody R_Qilnq_ulstoed b'f (priOI); 0~~~: J 'gl\atura: ' 1 F eceo.ed by (prim): Datcfl"!!l~EJ: Signature:
/;AI-r-;,.,._ PA-1-.u-"'J%H3 liDO f.,-.uZ"_ PJ.A.A. Record RC:iflq~llod b'f (prlm): OulefTlmlr. Sigr>attn-« R~N!ld by (pnntJ: om11(Time' Signature:
MUSTber------------------------------1~~~~~~~~----~~~------1 Signed Sample Disposal: Return to Client: lab Olspceal: ~ew ~ 1 ') CJO ;. ~ ....... ~Rietllme: L(__ L.( .-L ~ :;~~: { c._--
ln certain circumstances, samples submitted to Energy laboratories, Inc. may be subcontracted 1e 0~81' certified laboratories in order to complete the analysis requested.
This serves as notice of this possibility. All sub-contract data will beCiearly notated on your analytical report. , ·-.:=-.. --•: ..... -~ ..... u,"l"~n"3hlo fcc c::"hAI'iuiP. fnrms. and links.
EI\ERGY
I d i ·l
www.energytab.com
AM/ftJal~ ... 1111
Helena, MT 877-472-0711 • Billings, MT BGI-735-4488 • Caspar, WV a&l-235-1515
Glllatta, WY 188-188-7175 • Rapid City, SD 818-812-1225 • Collage Station, 1X 881-680-2218
August 17, 2013
Energy Fuels Resources (USA) Inc
225 Union Blvd Ste 600
Lakewood, CO 80228-1826
Workorder No.: C13070231
ANAL VTICAL SUMMARY REPORT
Project Name: 2nd Quarter Air 2013
Energy Laboratories, Inc. Casper WY received the following 6 samples for Energy Fuels Resources (USA) Inc on 7/8/2013 for
analysis.
Sample ID Client Sample ID Collect Date Receive Date Matrix Test
C13070231-001 BHV-1 07/02/13 00:00 07/08/13 Filter Composite of two or more samples
Metals, Total
Digestion, Total Metals
Lead 210
Radium 226
Thorium, Isotopic
C13070231-002 BHV-2 07/02/13 00:00 07/08/13 Filter Same As Above
C13070231-003 BHV-4 07/02/13 00:00 07/08/13 Filter Same As Above
C13070231-004 BHV-5 07/02/13 00:00 07/08/13 Filter Same As Above
C13070231-005 BHV-6 07/02/13 00:00 07/08/13 Filter Same As Above
C 13070231-006 Blank 07/02/13 00:00 07/08/13 Filter Same As Above
The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were
performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted.
Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601,
unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical
Report, the QA/QC Summary Report, or the Case Narrative.
If you have any questions regarding these test results, please call.
Report Approved By:
Digitally signed by
Steve Carlston ~rb--~ Date: 2013.08.17 17:43:27 -06:00
· Interim Branch Manager
Page 1 of 22
EN:RGY ,· -· i
, , I '•·l '-
www.energylab.com ..,.,_.......,.,,. Helena, MT 877-412-0711 • Billings, MT 800-735·4481 • Caspar, WY 888-235-0515
Gillette WY 886·888·7175 • Ra ld Cl SO 888-872-1225 • Collo 11 Station TX 888·690-2218
CLIENT: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Air 2013
Sample Delivery Group: C13070231
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Report Date: 08/17/13
CASE NARRATIVE
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are
hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has
begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for
seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria
for PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize
its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b -Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h-Energy Laboratories, Inc.-Helena, MT
eli-r-Energy Laboratories, Inc. -Rapid City, SD
eli-cs -Energy Laboratories, Inc. -College Station, TX
CERTIFICATIONS:
US EPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641 , Radiochemical E871 017; California: 02118CA;
Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify ELl's certification coverage by visiting www.energylab.com
ELl appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College
Station, TX, EPA Number TX01520.
Page 2 of22
www.anerolab.com
AMITIIal ~.fila /liZ
Helena, MT 177-472-0711 • Billings, MT BDD-735-4489 • Gasper, WY 888-235-0515
Gillette, WY 8&6-&81-7175 • Rapid City, SD 888-&72-1225 • Collage Station, 1X 888-690-2218
HIGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: August 17,2013
PROJECT: 2nd Quarter Air 2013
SAMPLE ID: BHV-1
Quarter/Date Sampled Concentration
Air Volume Radionuclide !JCi/mL
Cl3040210-001 ""u 9.91E-16
First Quarter 2013 23oTh 1.86E-16
Air Volume in mLs 226Ra 2.04E-16
1.36E+11 210Pb 1.82E-14
Quarter/Date Sampled Concentration
Air Volume Radionuclide !JCilmL
C 13070231-00 I ""U 1.46E-15
Second Quarter 2013 230Th 3.34E-16
Air Volume in mLs 226Ra 3.91E-16
1.34E+Il 210Ph 5.78E-15
+LLD's are from Reg. Guide 4.14
Counting
Precision
!JCi/mL
N/A
5E-17
IE-17
2E-16
Counting
Precision
!JCi/mL
N/A
5E-17
2E-17
IE-16
*Effluent Concentration from the NEW I 0 CFR Part 20 -Appendix B -Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDC !JCilmL
N/A
2E-17
4E-18
5E-17
MDC !JCilmL
N/A
2E-17
3E-18
6E-17
-
L.L.D.+ Effluent Cone.* %Effluent
!JCi/mL !JCi/mL Concentration
IE-16 9E-14 l.IOE+OO
1E-16 3E-14 6.21E-01
IE-16 9E-13 2.27E-02
2E-15 6E-13 3.03E+00
L.L.D.+ Effluent Cone.* % Etlluent
!JCilmL !JCilmL Concentration
1E-16 9E-14 1.62E+OO
IE-16 3E-14 l.llE+OO
1E-16 9E-13 4.35E-02
2E-15 6E-13 9.64E-01
Page 3 of 22
www.energytab.com EN:RGY
' < ' •I , ' I •• II AM/tflf:al Elcelllsl Sllu 1HZ
Helena, MT 871·412·0711 • Billings, MT 800·735·4489 • Casper, WY 888-235-1515
Gillatta, WY 188-888-7115 • Rapid City, SD 888-672-1225 • Collage Station, TX 888-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Air 2013
Lab ID: c 13070231-001
Client Sample ID BHV-1
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 210 precision(±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
0.288 mg/filter
195 pCiiFilter
774 pCiiFilter
19 pCiiFilter
8.6 pCiiFilter
52.3 pCiiFilter
2.1 pCiiFilter
0.4 pCiiFilter
45 pCiiFilter
6.7 pCiiFilter
2.2 pCiiFilter
MDC -Minimum detectcble concentration
Qualifiers
MCU
RL QCL
0.0003
0.2
Report Date: 08/17/13
Collection Date: 07/02/13
DateReceived: 07/08/13
Matrix: Filter
Method Analysis Date I By
SW6020 08107113 04:24 I cp
SW6020 08107113 04:24 I cp
E909.0 08109113 23:22 I eli-cs
E909.0 08109113 23:22 I eli-cs
E909.0 08109113 23:22 I eli-cs
E903.0 0712311313:1411mc
E903.0 0712311313:1411mc
E903.0 0712311313:1411mc
E908.0 07/18113 18:23 I dmf
E908.0 07118113 18:23 I dmf
E908.0 07118113 18:23 I dmf
MCL -Maximum contaminant level.
ND-Not detected at the reporting limit.
Page 4 of 22
www.energylab.com
AM/yllal Elullltlu ~ 1151
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-&8&-7175 • Rapid City, SO BBB-612-1225 • College Station, TX 888-690-221 B
HIGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: August 17,2013
PROJECT: 2nd Quarter Air 2013
SAMPLE ID: BHV-2
Quarterillate Sampled Concentration Radionuclide Air Volume J!CilmL
c 1304021 0-002 ""U 3.38E-16
First Quarter 2013 23oTh 3.94E-17
Air Volume in mLs 226Ra 8.32E-17
1.36E+11 210Pb 1.42E-14
Quarterillate Sampled Concentration Radio nuclide Air Volume J!CilmL
c 13070231-002 nalu 4.06E-16
Second Quarter 20 13 230Th 4.89E-17
Air Volume in mLs 226Ra 8.06E-17
1.38E+ll 210Pb 4.93E-15
+LLD's are from Reg. Guide 4.14
Counting
Precision
J!CilmL
N/A
IE-17
9E-18
2E-16
Counting
Precision
J!CilrnL
N/A
IE-17
7E-18
lE-16
*Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDC J!CilmL
N/A
9E-18
4E-18
SE-17
MDC J!CilmL
N/A
6E-18
3E-18
6E-17
L.L.D.+ Effluent Cone.* % Etlluent
J1CilmL J!Ci/rnL Concentration
IE-16 9E-14 3.75E-OI
IE-16 3E-14 1.31E-OI
1E-16 9E-13 9.25E-03
2E-15 6E-13 2.37E+00
L.L.D.+ Effluent Cone.* %Effluent
J1CilmL J!CilrnL Concentration
1E-16 9E-14 4.51E-01
lE-16 3E-14 l.63E-01
1E-16 9E-!3 8.95E-03
2E-15 6E-13 8.21E-OI
Page 5 of 22
EN:RGY
"I• •I · •
www.energylab.com
AMiyflat~Sotrar 11!1
Helena, MT 877-472-0711 • Billings, MT 800-735·4489 • Casper, WY 888-235-0515
Gillette, WY 816-686-7175 • Rapid City, SD 888-672-1225 • College Station, 1X 888-680-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Air 2013
Lab 10: c 13070231-002
Client Sample ID BHV-2
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
0.0827 mg/filter
56.0 pCiiFilter
679 pCiiFilter
18 pCiiFilter
8.6 pCiiFilter
11 .1 pCiiFilter
pCi/Filter
0.4 pCi/Filter
6.7 pCi/Filter
1.5 pCi/Filter
0.88 pCi/Filter
MDC -Minimum detectable concentration
Qualifiers
MCU
RL QCL
0.0003
0.2
Report Date: 08/17/13
Collection Date: 07/02/13
DateReceived: 07/08/13
Matrix: Filter
Method Analysis Date I By
SW6020 08/07113 04:51 I cp
SW6020 08107/13 04:51 I cp
E909.0 08/10/13 00:31 I eli-cs
E909.0 08/10/13 00:31 I eli-cs
E909.0 08/10/13 00:31 I eli-cs
E903.0 07/23/13 16:11 lime
E903.0 07/23/1316:11/lmc
E903.0 07/23/13 16:11 lime
E908.0 07/18/1318:23 /dmf
E908.0 07/18/1318:23 /dmf
E908.0 07/18/1318:23 /dmf
MCL -Maximum contaminant level.
NO-Not detected at the reporting limit.
Page 6 of 22
EI\ERGY
•' 1 I
www.energylab.com
AII/Jfklll ElUIIHu Sl"" liSt
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218
.. HIGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: August 17,2013
PROJECT: 2nd Quarter Air 2013
SAMPLEID: BHV-4
Quarter/Date Sampled Concentration
Air Volume Radionuclide J1CilmL
c !304021 0-003 ""'U 3.04E-15
First Quarter 2013 z3oTh 4.99E-16
Air Volume in mLs 226Ra 2.79E-16
1.35E+ll 210Pb 2.13E-14
Quarter/Date Sampled Concentration I Radionuclide Air Volume J1CilrnL
c 13070231-003 ""'u 2.50E-15
Second Quarter 2013 230Th 3.62E-16
Air Volume in mLs 226Ra 2.40E-16
1.37E+ll zwPb 4.93E-15
+LLD's are from Reg. Guide 4.14
Counting
Precision
J1CilrnL
N/A
9E-17
2E-17
2E-16
Counting
Precision
J1CilrnL
N/A
SE-17
IE-17
IE-16
*Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDC J1CilrnL
N/A
2E-17
4E-18
SE-17
MDC J1CilrnL
N/A
IE-17
3E-18
6E-17
L.L.D.+ Effluent Cone.* % Efnuent
J1CilrnL J1CilmL Concentration
IE-16 9E-14 3.38E+00
IE-16 3E-14 1.66E+00
IE-16 9E-!3 3.10E-02
2E-15 6E-13 3.54E+OO
L.L.D.+ Effluent Cone.* %Effluent
J1CilmL J1CilrnL Concentration
IE-16 9E-14 2.78E+00
IE-16 3E-14 1.21E+OO
IE-16 9E-13 2.67E-02
2E-15 6E-13 8.22E-Ol
Page 7 of 22
r www.energylab.com EN:RGY
~, • t • • • J I ~~Sitluii!Z
Helena, MT 877·412·0711 • Billings, MT 800·735-4489 • Casper, WY 888·235-1515
Gillette, WY 865-688-7115 • Rapid City, SD 818-&72-1225 • Collage Station, TX 888-680-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Air 2013
Lab ID: C13070231-003
Client Sample ID BHV-4
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 210 precision (±)
Lead 210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL-Quality control limit.
Result Units
0.507 mg/filter
343 pCiiFilter
677 pCiiFilter
18 pCi/Filter
8.5 pCiiFilter
32.9 pCi/Filter
1.6 pCii Filter
0.4 pCiiFilter
50 pCii Filter
6.9 pCii Filter
1.7 pCii Filter
MDC -Minimum detectcble concentration
Qualifiers
MCU
RL QCL
0.0003
0.2
Report Date: 08/17/13
Collection Date: 07/02/13
DateReceived: 07/08/13
Matrix: Filter
Method Analysis Date I By
SW6020 08107/13 04:55 / cp
SW6020 08/07/13 04:55 / cp
E909.0 08/10/13 01 :40 I eli-cs
E909.0 08/10113 01 :40 I eli-cs
E909.0 08110113 01 :40 I eli-cs
E903.0 07123113 16:11 I lmc
E903.0 07123113 16:11 lime
E903.0 07/23/13 16:11/lmc
E908.0 07/18113 18:23 I dmf
E908.0 07118113 18:23 I dmf
E908.0 07118113 18:23 I dmf
MCL -Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 8 of 22
www.energylab.com
ADI/JIIU/ EluiiNu Slta 1151
Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-&B&-7175 • Rapid City, SD BBB-&72-1225 • College Station, TX 888-&90-2218
HIGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: August 17,2013
PROJECT: 2nd Quarter Air 2013
SAMPLE ID: BHV-5
Quarter/Date Sampled Concentration
Air Volume Radionuclide J.1Ci/mL
c 1304021 0-004 ""U 6.66E-15
First Quarter 2013 23oTh 1.48E-15
Air Volume in mLs 226Ra 1.12E-15
l.35E+ll 210Pb l.SOE-14
Quarter/Date Sampled Concentration Radio nuclide Air Volume J.1CilmL
c 13070231-004 ""u 7.35E-15
Second Quarter 2013 23'111 1.72E-15
Air Volume in mLs 226Ra 2.02E-15
l.37E+ll 210Pb 6.67E-15
+LLD's are from Reg. Guide 4.14
Counting
Precision
JlCi/mL
N/A
3E-16
3E-17
2E-16
Counting
Precision
J.1Ci/mL
N/A
2E-16
4E-17
IE-16
*Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDC J.1CilmL
N/A
4E-17
4E-18
SE-17
MDCJ.1CilmL
N/A
2E-17
3E-18
6E-17
L.L.D.+ Effluent Cone.* %Effluent
J.1CilmL J.1CilmL Concentration
1E-16 9E-14 7.40E+OO
1E-16 3E-14 4.95E+00
1E-16 9E-13 1.24E-01
2E-15 6E-13 3.00E+OO
L.L.D.+ Effluent Cone.* %Effluent
J.1Ci/mL J.1CilmL Concentration
IE-16 9E-14 8.16E+00
IE-16 3E-14 5.74E+00
1E-16 9E-13 2.25E-01
2E-15 6E-l3 1.11E+00
Page 9 of 22
www.energylab.com EN:RGY
I ·I· I '"j . ANI1fltM ~ Sllu J/ISZ
Helena, MT 877·412-0711 • Billings, MT 801·735·4489 • Casper, W'{ 888·235-1515
Gillette, W'{ 88&-186-7175 • Rapid City, SO 118-872-1225 • College Station, TX 888-610-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Air 2013
LabiD: c 13070231-004
Client Sample ID BHV-5
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 210 precision (±)
Lead 210MDC
Radium226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL -Quality control limit.
Result Units
1.49 mglfilter
1010 pCiiFilter
917 pCiiFilter
20 pCiiFilter
8.6 pCiiFilter
278 pCiiFilter
4.8 pCiiFilter
0.4 pCiiFilter
237 pCiiFilter
25 pCiiFilter
3.0 pCiiFilter
MDC -Minimum detectable concentration
Qualifiers
MCU
RL OCL
0.0003
0.2
Report Date: 08/17/13
Collection Date: 07/02/13
DateReceived: 07/08/13
Matrix: Filter
Method Analysis Date I By
SW6020 08107113 04:59 I cp
SW6020 08107113 04:59 I cp
E909.0 08110113 02:50 I eli-cs
E909.0 08110113 02:50 I eli-cs
E909.0 08110113 02:50 I eli-cs
E903.0 07123113 16:11 lime
E903.0 07123113 16:11 I lmc
E903.0 07123113 16:11 I lmc
E908.0 07118113 18:23 I dmf
E908.0 07118113 18:23 I dmf
E908.0 07118113 18:23 I dmf
MCL-Maximum contaminant level.
ND -Not detected at the reporting limit.
Page 10 of 22
EI\ERGY
'~ • • I '
www.energylab.com
Ani/fila/ Ur:lllltlu Slla 11$2
Helena, MT 177-472-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 866-686-7175 • Rapid City, SD 818-&72-1225 • College Station, TX 888-&90-2218
HIGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: August 17,2013
PROJECT: 2nd Quarter Air 2013
SAMPLE ID: BHV-6
Quarter/Date Sampled Concentration
Air Volume Radionuclide pCi/mL
c 1304021 0-005 ""'u 4.52E-15
First Quarter 2013 23oTh 7.93E-16
Air Volume in mLs 226Ra 4.91E-16
1.35E+11 zwPb 1.70E-14
Quarter/Date Sampled Concentration Radionuclide Air Volume pCilmL
c 13070231-005 natu 5.91E-15
Second Quarter 20 13 23~ 6.74E-16
Air Volume in mLs 226Ra 7.85E-16
1.37E+11 zwPb 5.18E-15
+LLD's are from Reg. Guide 4.14
Counting
Precision
pCi/mL
N/A
2E-16
2E-17
2E-16
Counting
Precision
pCi!mL
N/A
9E-17
2E-17
IE-16
*Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDCJ.!CilmL
N/A
4E-17
4E-18
6E-17
MDC pCilmL
N/A
2E-17
3E-18
6E-17
L.L.D.+ Effluent Cone.* %Effluent
pCi/mL pCilmL Concentration
1E-16 9E-14 5.02E+00
IE-16 3E-14 2.64E+00
IE-16 9E-13 5.46E-02
2E-15 6E-13 2.83E+00
L.L.D.+ Effluent Cone.* %Effluent
J.!CilmL pCilmL Concentration
IE-16 9E-14 6.57E+OO
1E-16 3E-14 2.25E+00
1E-16 9E-13 8.73E-02
2E-15 6E-13 8.64E-01
Page 11 of 22
EI\ERGY
, . · • ~) '1 . f ·I
www.enerRYtab.com
IM/fbiEzaiiMt:l S1IIU 11!1
Helena, MT 877-472-0711 • Billings, MT 801-735-4489 • Casper, WY 888-235-1515
Gillette, WV 116-686-7175 • Rapid Crty, SD 188-872-1225 • Collage Station, TX 888-610-2211
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Air 2013
LabiD: c 13070231-005
Client Sample ID BHV-6
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 21 0 precision (±)
Lead210MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL -Analyte reporting limit.
QCL -Quality control limit.
Result Units
1.20 mg/filter
812 pCi/Filter
712 pCi/Filter
18 pCi/Filter
8.5 pCi/Filter
108 pCi/Filter
3.0 pCi/Filter
0.4 pCi/Filter
93 pCi/Filter
12 pCi/Filter
3.1 pCi/Filter
MDC -Minimum detectable concentration
Qualifiers
MCU
RL QCL
0.0003
0.2
Report Date: 08/17/13
Collection Date: 07/02/13
DateReceived: 07/08/13
Matrix: Filter
Method Analysis Date I By
SW6020 08/07/13 05:04 / cp
SW6020 08/07/13 05:04 I cp
E909.0 08/1 0/13 03:59/ eli-cs
E909.0 08/1 0/13 03:59 / eli-cs
E909.0 08/10/13 03:59/ eli-cs
E903.0 07/23/1316:11 lime
E903.0 07/23/13 16:11 /lmc
E903.0 07/23/13 16:11 /lmc
E908.0 07/18/13 18:23 / dmf
E908.0 07/18/13 18:23 / dmf
E908.0 07/18/1318:23 /dmf
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
Page 12 of22
EI\ERGY www.energylab.com
AIM/ft/UI EIA"--Slta IIU
Helena, hfT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillette, WY 8&&-&8&-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-&90-2218
I HIGH VOLUME AIR SAMPLING REPORT
CLIENT: Energy Fuels Resources (USA) Inc
REPORT DATE: August 17,2013
PROJECT: 2nd Quarter Air 2013 •
SAMPLE ID: Blank
Quarter/Date Sampled Concentration
Air Volume Radio nuclide JiCilmL
c 13040210-006 nalu 9.60E-18
First Quarter 20 13 230Th 3.27E-18
Air Volume in mLs 226Ra 3.89E-18
1.36E+I1 2JOPh -4.09E-17
•
Counting
Precision
JiCilmL
N/A
3E-18
3E-18
3E-17
N ote: Th IS'Sllmp c uses ">' o a1r vo orne Ll6 000 000 L f ' or companson purpo,~cs.
Quarter/Date Sampled Concentration Counting
Radio nuclide Precision Air Volume JiCi/mL JiCilmL
c 13070231-006 ""U 7.23E-18 N/A
Second Quarter 20 13 230Th 7.06E-18 2E-18
Air Volume in mLs 22C>Ra 4.52E-18 2E-18
1.36E+11 210Pb -7.38E-18 4E-17
Note: This sample uses 136,000,000 L of air volume for comparison purposes.
+LLD's are from Reg. Guide 4.14
*Effluent Concentration from the NEW 10 CFR Part 20-Appendix B-Table 2
Year for Natural Uranium
Year for Thorium-230
Week for Radium-226
Day for Lead-210
MDC JiCilmL
N/A
6E-18
4E-18
SE-17
MDC JiCilmL
N/A
2E-18
3E-18
6E-17
--~
L.L.D.+ Effluent Cone.* %Effluent
JiCi/mL JiCi/mL Concentration
IE-16 9E-14 1.07E-02
LE-16 3E-14 1.09E-02
IE-16 9E-13 4.32E-04
2E-15 6E-13 -6.82E-03
L.L.D.+ Effluent Cone.* %Effluent
11CilmL JiCilmL Concentration
IE-16 9E-14 8.03E-03
IE-16 3E-14 2.35E-02
IE-16 9E-13 5.02E-04
2E-15 6E-13 -1.23E-03
Page 13 of 22
El\ERGY
I < ; o o '!I
www.ooerRYtab.com
~EBe/lelu Sllcl IIU
Helena, MT 877-472-0711 • Billings, MT 801-735·4419 • Casper, W't 888-235-1515
Gillette, W't 11&-186-7175 • Rapid City, SD 88&-172-1225 • College Station, TX 888-610-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Air 2013
Lab ID: C13070231-006
Client Sample ID Blank
Analyses
TRACE METALS
Uranium
Uranium, Activity
RADIONUCLIDES
Lead 210
Lead 210 precision(±)
Lead210 MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL -Quality control limit.
Result Units
0.0015 mg/filter
1.0 pCi/Filter
-1 pCi/Filter
5.1 pCi/Filter
8.6 pCi/Filter
0.6 pCiiFilter
0.3 pCiiFilter
0.4 pCiiFilter
0.96 pCiiFilter
0.31 pCiiFilter
0.21 pCi/Filter
MDC -Minimum detectable concentration
Qualifiers
u
MCU
RL QCL
0.0003
0.2
Report Date: 08/17/13
Collection Date: 07/02/13
DateReceived: 07/08/13
Matrix: Filter
Method Analysis Date I By
SW6020 08/07/13 05:08/ cp
SW6020 08/07/13 05:08/ cp
E909.0 08/1 0/13 05:08 I eli-cs
E909.0 08/1 0/13 05:08 I eli-cs
E909.0 08/1 0/13 05:08/ eli-cs
E903.0 07/23/13 16:11/lmc
E903.0 07123113 16:11 /lmc
E903.0 07123113 16:11 I lmc
E908.0 07118113 18:23/ dmf
E908.0 07/18113 18:23/ dmf
E908.0 07/18/13 18:23/ dmf
MCL-Maximum contaminant level.
ND -Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Page 14 of 22
EI\ERGY
I •# ! I I 'I • I
www.energylab.com
AMiyllal El:clllww Sllu lllf2
Helena, MTB77-472-0711 • Billings, MT BG0-735·4489 • Casper, WY 888-235-1515
Gillatta, WY 818-188-7175 • Rapid City, SD 888-172-1225 • College Station, TX 888-690-2218
QAJQC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Air 2013
Analyte
Method: E903.0
Sample ID: LCS-381 07
Radium 226
Sample ID: MB-38107
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Sample ID: C13070231-001AMS
Radium 226
Sample ID: C13070231·001AMSD
Radium 226
Qualifiers:
RL -Analyte reporting limit.
Count Result Units
Laboratory Control Sample
23.4 pCi/Filter
3 Method Blank
0.2 pCi/Filter
0.2 pCi/Filter
0.3 pCi/Filter
Sample Matrix Spike
126 pCi/Filter
Sample Matrix Spike Duplicate
131 pCi/Filter
MDC -Minimum detectable concentration
Report Date: 08/17/13
Work Order: C13070231
RL %REC Low Limit High Limit RPD RPDLimit Qual
Run: BERTHOLD 770·1_130717A
108 80 120
Run: BERTHOLD 770-1_130717A
Run: BERTHOLD 770·1 _130717A
103 70 130
Run: BERTHOLD 770·1 _130717A
110 70 130 3.8
ND-Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Batch: R176249
07/23/13 13:14
07/23/13 13:14
u
07/23/13 16:11
07/23/13 16:11
17.5
Page 15 of 22
EN:RGY
#' I• •I •'•I ,ll '
www.energytab.com
AMiytlrM ~ Slta 71152
Helena, MT 877·472·0111 • Billings, MT 800·735-4489 • Casper, WY 888·235·0515
Gillette, WY 81&-686· 7175 • Rapid City, SD 88&-&72·1225 • College Station, TX 888-690-2218
QAIQC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Air 2013
Analyte
Method: E908.0
Sample ID: C13070098-004AMS
Thorium 230
Sample ID: C13070098-004AMSD
Thorium 230
Sample ID: LCS-38191
Thorium 230
Sample ID: MB-38191
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Qualifiers:
RL-Analyte reporting limit.
Count Result Units
Sample Matrix Spike
115 pCi/Filter
Sample Matrix Spike Duplicate
123 pCi/Filter
Laboratory Control Sample
18.3 pCi/Filter
3 Method Blank
0.2 pCi/Filter
0.1 pCi/Filter
0.2 pCi/Filter
MDC -Minimum detectable concentration
Report Date: 08/1 7 I 13
Work Order: C13070231
RL %REC Low Limit High Limit RPD RPDLimit Qual
Run: ALPHANALYST_130715C
108 70 130
Run: ALPHANAL YST _130715C
115 70 130 6.3.
Run: ALPHANAL YST _130715C
108 80 120
Run: ALPHANAL YST _130715C
ND -Not detected at the reporting limit.
Batch: R176720
07/18/13 18:22
07/18/1318:22
30.3
07/18/13 18:23
07/18/13 18:23
Page 16 of 22
www.ener&Yiab.com
AM/fib/ ElrtliJwa Sltlu 1152
Helena, MT 877-472-0711 • Billings, MT 880-735-4489 • Casper, WY 888-235-8515
Gilletta, WY 81&-181-7175 • Rapid City, SD 888-172-1225 • College Station, TX 881-610-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Air 2013
Analyte Count Result
Method: E909.0
Units
SampleiD: LCS-19226 Laboratory Control Sample
Lead 210 87.0 pCi/Filter
RL %REC
64
Report Date: 08/17/13
Work Order: C13070231
Low Limit High Limit RPD RPDLimit Qual
Batch: T _19226
Run: SUB-T52308 08/09/13 17:35
80 120 s
-LCS response is outside of the acceptance range for this analysis. Since the MB, MS. and MSD are acceptable the batch is approved.
Sample ID: MB-19226 3 Method Blank Run: SUB-T52308 08/09/13 18 :44
Lead 210 2 pCi/Filter u
Lead 21 0 precision (±) 5 pCi/Filter
Lead 210 MDC 9 pCi/Filter
Sample ID: C13070233-001AMS Sample Matrix Spike Run: SUB-T52308 08/09/13 21 :03
Lead 210 2.92E-05 pCi/Filter 117 70 130
Sample ID: C13070233-001 AM SO Sample Matrix Spike Duplicate Run: SUB-T52308 08/09/13 22:12
Lead 210 2.75E-05 pCi/Filter 100 70 130 6.1 17.2
Qualifiers:
RL-Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration S -Spike recovery outside of advisory limits.
U -Not detected at minimum detectable concentration
Page 17 of 22
EI'ERGY www.energylab.com Helena, MT 877-472·0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515
Gillatta, WY 86&-686-7175 • Rapid City, SD 818-672-1225 • College Station, IX 881-690-2218 ~·· ·---1 l I "• I ': I AIMiyflt:M ~ Sll!u 11!2
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Air 2013
Report Date: 08/17/13
Work Order: C13070231
Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual
Method: SW6020
SampleiD: ICV
Uranium
SampleiD: ICSA
Uranium
Sample ID: ICSAB
Uranium
Method: SW6020
Sample ID: MB-38219
Uranium
SampleiD: LCS2-38219
Uranium
Initial Calibration Verification Standard
0.0506 mg/L 0.00030
Interference Check Sample A
2.68E-05 mg/L 0.00030
Interference Check Sample AB
9.90E-06 mg/L 0.00030
Method Blank
7E-05 mg/filter 4E-05
Laboratory Control Sample
0.0746 mg/filter 0.00030
101
Analytical Run: ICPMS4-C_130806A
08/06/13 14:22
90 110
Run: ICPMS4-C_130806A
Run: ICPMS4-C_130806A
08/06/13 14:27
08/06/13 14:31
Batch: 38219
08/07/13 04:11
149 85 115
08/07/13 04:15
s
-Response is above standard QA limit. This could indicate a high bias for the sample results. Insufficient sample remains to perform are-digestion. Re-analysis of
samples confirms data, and instrument QC meets criteria, so this batch is approved.
Sample ID: C13070231-001ASD 2 Serial Dilution Run: ICPMS4-C_130806A 08/07/13 04:47
Uranium 0.249 mg/filter 0.00030 15 20
Uranium, Activity 168 pCi/Filter 0.20 0 0
Sample ID: C 13070233-001 AM S Sample Matrix Spike Run: ICPMS4-C_130806A 08/07/13 05:17
Uranium 0.271 mg/filter 0.00030 112 75 125
Sample ID: C 13070233·001 AM SO Sample Matrix Spike Duplicate Run: ICPMS4-C_130806A 08/07/13 05:21
Uranium 0.271 mg/filter 0.00030 112 75 125 0.1 20
Qualifiers:
RL-Analyte reporting limit. ND -Not detected at the reporting limit.
MDC -Minimum detectable concentration S-Spike recovery outside of advisory limits.
Page 18 of 22
EI\ERGY
' I I 1
Helene, MT 877-472-0711 • Billings, MT BIID-735-4489 • Casper, WY 818-235-0515
Gillette, WY 811-181-7115 • Rapid City, SD 118-172-1225 • College Station, TX 888-&80-2218
Standard Reporting Procedures
Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual
Chlorine, are qualified as being analyzed outside of recommended holding time.
Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -<:try.
For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis.
Workorder Receipt Checklist
Energy Fuels Resources (USA) Inc
Login completed by: Corinne Wagner
Reviewed by: Bl2000\kmiller
Reviewed Date: 7/9/2013
Shipping container/cooler in good condition?
Custody seals intact on all shipping container(s)/cooler(s)?
Custody seals intact on all sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples In proper container/bettie?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
(Exclude analyses that are considered field parameters
such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.)
Temp Blank received in all shipping container(s)/cooler(s)?
Container/Temp Blank temperature:
Water· VOA vials have zero headspace?
Water· pH acceptable upon receipt?
Contact and Corrective Action Comments:
None
Yes 0
Yes D
Yes D
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes D
N/A'C
Yes D
Yes D
C13070231
Date Received: 7/8/2013
Received by: CAV
Carrier Ground
name:
No 0
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
NoD
No 0
Not Present 0
Not Present 0
Not Present 0
Not Applicable 0
No VOA vials submitted 0
Not Applicable 0
Page 19 of 22
Sheet 1 of 1
CHAIN OF CUSTODY
Samples Shipped to: Energy Laboratories Contact: Garrin Palmer -=2~39~3:"!S!=-a~lt;;;.:C~r..;.;:ee;;;;;k::....;.H;.:;.wy.;;;...._____ Ph: 435 678 2108
Casper WY 82601 gpalmer@ enerqvtuels.com
Chain of Custody/Sampling Analysis Request
Project
2nd Quarter Air
SampleiD
BHV-1
BHV-2
BHV-4
BHV-5
BHV-6
Blank
Comments:
Relinquished By:(Signature)
/' -=>..,..t--u ............. ,.
Re lnquished By:(Signature
Date
Collected
4/1/13-7/2/13
4/1/13-7/2/13
4/1/13-7/2/13
4/1/13-7/2/13
4/1113-7/2/13
4/1/13-7/2/13
Samplera Name Sampler-s Signature
Garrin Palmer 6--= p~
Time
Collected Laboratory Analysis Requested
na U-NAT, Th-230, Ra-226, Pb-210
na U-NAT, Th-230, Ra-226, Pb-21 0
na U-NAT, Th-230, Ra-226, Pb-21 0
na U-NAT, Th-230, Ra-226 Pb-210
na U-NAT. Th-230, Ra-226, Pb-210
na U-NAT, Th-230, Ra-226 Pb-210
Date/Time Received By:·(Signature)
7/3/2013
Date/Time
1100
Ci3D7o;23'
Page 20 of 22
ATTACHMENT D
AIR PARTICULATE LOADING GRAPHS AND SUPPORTING DATA
0 0 0 !=> ....
0 0 0 .... 0
0 0 .... 0 0
0 .... 0 0 0 .... 0 0 0 0
1/5/2009
3/5/2009
5/5/2009
7/5/2009
9/5/2009
11/5/2009
1/5/2010
+
)>
3/5/2010 -· """"
CJ ~
:I: 5/5/2010 r+
< • Q)
I .... r+ -· 7/5/2010
+
0
::::J
CJ 9/5/2010 "'0
:I: Q)
< I 11/5/2010 """" N r+ -· n
+ 1/5/2011 c -Q)
CJ :I: 3/5/2011 r+
< tO
I ~ r-
+
5/5/2011 0
Q)
7/5/2011 c.
CJ -:I: ::::J < I 9/5/2011 OQ
l.n -
+ 11/5/2011
,.. 3
OQ
CJ ""' :I: 1/5/2012 -3 < I C7\ w
3/5/2012 -
5/5/2012
7/5/2012
9/5/2012
11/5/2012
1/5/2013
3/5/2013
5/5/2013
0 0 9 f-'
0 0 f-' 0
0 f-' 0 0
f-' 0 0 0
0 0 0 0
1/5/2009
3/5/2009
5/5/2009
7/5/2009 -
9/5/2009
11/5/2009
1/5/2010
3/5/2010 "I -=-=-~ I I ~
~ I I :::I:
5/5/2010 1 I ~ < I
7/5/2010 ~ I ......... I I ......
"'0
I ~ I I OJ 9/5/2010 ~ ~ -· 11/5/2010 -n c: -
+
OJ 1/5/2011 r1' tO
OJ 3/5/2011 r-I < 0 I f-' OJ 5/5/2011 a. -·
7/5/2011 -j I _. .. • I I :::J -m O'Q -9/5/2011 -j ~ I I 3
O'Q
11/5/2011 -l • • J • I I ........ • 3
1/5/2012 -l -.t::t::: • I I w -
3/5/2012
5/5/2012 -
7/5/2012
9/5/2012 -
11/5/2012 -
1/5/2013
3/5/2013
5/5/2013
0 0 !=> ......
0 0 ...... 0
0 ...... 0 0 ...... 0 0 0 0 0 0 0
1/5/2009
3/5/2009
5/5/2009
7/5/2009
9/5/2009
11/5/2009
1/5/2010
3/5/2010 1 LE-= I I 0'
J I :I: 5/5/2010 -l I _ ...... • < I
7/5/2010 ·I I ~ I I N
-""0
I -_ .. I I QJ
9/5/2010 1 • ""'' r+ -· 11/5/2010 n c: -
+
QJ 1/5/2011 . r+ tD
OJ 3/5/2011 ,... I < 0 I N QJ 5/5/2011 c.. -·
7/5/2011 ·1 I ~~ • I I :::::J OQ -9/5/2011 i I• -=-I I 3 -OQ
11/5/2011 i . -_ ... I I ........ • 3
1/5/2012 ~ _r • I I w --
3/5/2012
5/5/2012
7/5/2012
9/5/2012
11/5/2012
1/5/2013
3/5/2013
5/5/2013 .,
0 0 0 !=' .....
0 0 0 ..... 0 0 0 ..... 0 0
0 ..... 0 0 0 ..... 0 0 0 0
1/5/2009
3/5/2009
5/5/2009
7/5/2009
9/5/2009
11/5/2009 -
1/5/2010
3/5/2010 -1 I ~~ I I ~
I .. -~ L I :I: 5/5/2010 1 I < I
7/5/2010 -1 I *" " ~ I I ~ .. .,
9/5/2010 -1 I I ~ I I QJ .., ,... -· n 11/5/2010 c -
+ 1/5/2011 QJ ,...
n> CJ r-I 3/5/2011 < 0 I ~ QJ 5/5/2011 ... Q. • -· ~, -:::::J 7/5/2011 1 I k :::::;;: Ill O'Q -9/5/2011 -1 I ._.,Ill .. I I 3
O'Q
11/5/2011 -1 I • ~ I I ........
~ 3
1/5/2012 -1 I ..... Ill p l h I I w -
3/5/2012
5/5/2012
7/5/2012 -
9/5/2012
11/5/2012
1/5/2013
3/5/2013
5/5/2013
0 0 !=> ....
0 0 .... 0
0 .... 0 0 .... 0 0 0
0 0 0 0
1/5/2009
3/5/2009
5/5/2009
7/5/2009
9/5/2009
11/5/2009
1/5/2010
3/5/2010 l ~-I I g,
I ::I:
5/5/2010 1 I ~--I_ < I
7/5/2010 1 I ~ I I U1
""C
I ~ I I OJ 9/5/2010 1 ~ -· 11/5/2010 n c -
+
OJ 1/5/2011 r+ 11)
OJ 3/5/2011 r-:I: < 0 I ll1 OJ 5/5/2011 c. -·
7/5/2011 1 r :a:-. I I ::l -OQ -9/5/2011 1 ~--I I 3
OQ
11/5/2011 1 .;:::;:::: . I I .......
3
1/5/2012 -1 •I :dl' I I w -
3/5/2012 -
5/5/2012 -1
7/5/2012 -
9/5/2012
11/5/2012
1/5/2013
3/5/2013
5/5/2013
0 0 !=' 1-"
0 0 1-" 0 0 1-" 0 0
1-" 0 0 0 0 0 0 0
1/5/2009
3/5/2009
5/5/2009
7/5/2009
9/5/2009
11/5/2009
1/5/2010
3/5/2010 l ~--I I OJ
I ~~-•. I I ::I:
5/5/2010 -1 < I
7/5/2010 -1 I ~· I I 0'\ .,
9/5/2010 --1 I --~ I I DJ .., ,.... -· 11/5/2010 n c: -
+ 1/5/2011 -DJ ,....
t1)
OJ
:I: 3/5/2011 r-< 0 Cn DJ 5/5/2011 c.. -·
7/5/2011 -l .. I ---__i:LS )( I I ::::J
OQ -9/5/2011 -l ~ "~ I I 3
OQ
11/5/2011 -1 )( 1=::-* }( I I ........
3
1/5/2012 ·I I~ I I w -
3/5/2012
5/5/2012
7/5/2012
9/5/2012
11/5/2012 -
1/5/2013
3/5/2013
5/5/2013
Period: December 31, 2013 through April1, 2013 (1st Quarter 2013) Page 1
BHV-1 on ::stream % 99.9% BHV-1 Total Volume: 4.81 E+06
Week Filter Start Stop Stop Start Total Total Loading, Per Cent
# Number Date Date Gross Tare Net Time Tim a Tlme Liters mufm3 On Stream SCFM
I 8399047 31-Dec-12 7-Jan-13 4.4332 4.3:125 0 1007 439~4.7 4~779.4 9916.2 t0.2~9.036 0 0098 98.4% 36.5
2 8399045 07-.Jan-1:1 14-J~n-13 4.4547 4.3534 0.1013 44111 .1 ~3944.7 10042 ~ 1{),522,076 0.0096 99.6% 37.0
3 8399036 14-Jan-13 21 -Jon-13 4.41 17 4.3455 0.0662 44281.5 441 t2.J 10167.6 10.652,832 0.0062 100 9'-;~, 37.0
4 8.199053 2 I -Jon-! 3 28-Jnn-13 4.4427 4 3249 0.1178 44448.2 4428 t.l 10021.2 I 0 499,445 0.0112 99.4% 37.0
5 8399027 2R-.Ian-13 4-Feb-1 3 4.3933 4 3253 n 0680 44616 8 44448 2 10116_6 10.599,398 0.0064 1004% 17.0
6 8399017 04-Feb-t3 11-Feb-13 <1.4 708 4.3221 0.1487 44782 4 44616.8 99396 10.413.951 0.0143 98.6% 37.0
7 8399015 11-Fcb-13 18-1-'ch-13 4.3515 4.2903 0.0612 44951.5 44782 4 10144 8 10,600.217 0.0058 100.6% .16.9
8 SJ9Y006 18-Feb-13 "5-Fcb-13 4.3938 4.3064 0.0874 45120.9 44951.5 10164.6 10.620.906 0.0082 1008% 36 9
C) 83990<n ~5-Frb-1.1 4-Mar-13 4.4220 4.l4n2 0 0758 452RR.6 45120.9 100~8 4 10.509,938 o.oon 99.R% 36.9
10 H399198 04-Mar-13 ll-Mar-13 4.4135 4.2830 0.1305 45455 5 45288.6 10018.8 10.383.450 0.0126 994% 36.6
II 839919 t 11 -Mnr-13 18-Mur-13 4.3.126 4,1949 0.1377 45612 4 45455 5 toOl 1.0 I 0.318.670 0.01.13 99.3% 36.4
12 8399 I 85 18-Mar-13 25-Mnl-13 4.4003 4.2271 0.1732 45789.9 45622.4 t004R.2 10.357.014 0.0167 99.7% 36.4
13 8399176 25-Mar-13 1-A£1-13 4.3579 4 1791 0,1788 45959.9 45789.9 10204.2 10,517.808 0.0170 t01.2% 36.4
Totals 91 2184.0 4.406 4.294669 0.1 I tJ 130854 t 36.244.74 I 0.0106 999% 36.8
BHV-2 on stream % BHV-2 Total Volume: 4.81 E+06
Week Filter Start Stop Stop Start Total Total Loading, Per Cent
# Number Date Date Gross Tare Net Time Time Time Liters mc/tn3 On Stream SCFM
1 8399048 31-Dec-12 07-Jan-13 4.5241 4.3490 0.1751 54146.7 53981.6 9907.8 t0,240,354 0,0171 98.3% 36.5
2 8399044 07-Jan-13 14-Jan-13 4.5572 4.3493 0.2079 54313.8 54146.7 10024.2 10,502,588 0.0198 99.4% 37.0
3 8399037 14-Jan-13 21-Jan-13 4.5472 4_3483 0 1989 54483.3 54313.8 10167.0 10,652,203 0.0187 100.9% 37.0
4 8399032 21-Jan-13 213-Jan-13 4.5671 4.3303 0.2368 54650.2 54483.3 10016.4 10,494,416 0.0226 99.4% 37.0
5 8399026 28-Jan-13 04-Feb-13 4.3899 4.3177 0.0722 54818.9 54650.2 10120 2 10,603,170 0.0068 100.4% 37.0
6 8399018 04-Feb-13 11 -Feb-13 4.5810 4.3179 0.2631 54984.6 54818.9 9940.8 10,415,208 0.0253 98.6% 37 0
7 8399014 11-Feb-13 18-Feb-13 4.3877 4.3176 0.0701 55152.0 54984.6 10047.6 10,498,653 0.0067 99.7% 36 9
8 8399007 18-Feb-13 25-Feb-13 4.4350 4.3250 0.1100 55323_1 55152.0 10262.4 10,723,096 0.0103 101.8% 36 9
9 8399002 25-Feb-13 04-Mar-13 4.4191 4.2805 0.1386 55490.4 55323.1 10038.6 10,489,249 0.0132 99.6% 36.9
10 8399197 04-Mar-13 11-Mar-13 4.2759 4.4979 -0.2220 55657,8 55490.4 10043.4 10,408,946 -0.0213 99.6% 36.6
11 8399191 11-Mar-13 18-Mar-13 4.3982 4,2348 0.1634 55824.6 55657.8 10009.2 10,316,815 0.0158 99.3% 36.4
12 8399181 18-Mar-13 25-Mar-13 4.5151 4.2452 0.2699 55992.0 55824.6 10048,2 10,357,014 0 0261 99.7% 36 4
13 8399177 25-Mar-13 01-Apr-13 4.4960 4.2105 0.2855 56162.3 55992.0 10217.4 10,531.414 0.0271 101.4% 36.4
Totals 91 2184.0 4.46873 4.31723 0.1515 130843.2 136.233.127 0.0145 99.8% 36.8
BHV-4 on stream % 99.2% BHV-4 Total Volume: 4.78E+06
Week Filter Start Stop Stop Start Total Total Loading, Per Cent
II Number Date Date Gross: Tace Net Time ·nme Time Liters mnlr1l3 On Stream SCFM
1 8399049 31-Dec-12 07-Jan-13 4.4796 4.3540 0.1256 29450_0 29284.5 9930 6 10,263,920 0 0122 98_5% 36,5
2 8399043 07-Jan-13 14-Jan-13 4.4460 4.3346 0.1114 29611.6 29450.0 9694.8 10,157,468 0.0110 96.2% 37.0
3 8399036 14-Jan-13 21-Jan-13 4.4400 4.3308 0.1092 29783.2 29611.6 10296.0 10,787,359 0.0101 102.1% 37.0
4 8399031 21-Jan-13 28-Jan-13 4.4430 4.3253 0.1177 29946.9 29783.2 9820.8 10,289,481 0.0114 97.4% 37 0
5 8399019 28-Jan-13 04-Feb-13 4.3106 4.2538 0.0568 30115.2 29946.9 10100.4 10,582,425 0.0054 100.2% 37 0
6 8399019 04-Feb-13 11-Feb-13 4 4275 4.3020 0.1255 30280,9 30115.2 9940.2 10,414,580 0.0121 98.6% 37 0
7 8399013 11-Feb-13 18-Feb-13 4.3794 4.3090 0.0704 30448.8 30280.9 10074.6 10,526,865 0.0067 99.9% 36 9
8 8399008 18-Feb-13 25-Feb-13 4,3980 4.2946 0.1034 30619.7 30448.8 10252.2 10,712,438 0.0097 101.7% 36,9
9 8399001 25-Feb-13 04-Mar-13 4.4162 4.3476 0.0686 30783.1 30619.7 9802.2 10,242,237 0.0067 97.2% 36.9
10 8399196 04-Mar-13 11-Mar-13 4.4274 4.2194 0.2080 30949.3 30783.1 9972_6 10,335,569 00201 98.9% 36,6
11 8399189 11-Mar-13 18-Mar-13 4.4060 4.2217 0.1843 31114.6 30949.3 9934.2 10,239,510 0,0180 98.6% 36.4
12 8399182 18-Mar-13 25-Mar-13 4.5054 4.2426 0.2628 31282.3 31114.8 t0049.4 10,358,251 0.0254 99.7% 36.4
13 8399178 25-Mar-13 01-Apr-13 4.3008 4.2209 0.0799 31452.0 31262.3 10178.4 10.491,215 0.0076 101.0% 36.4
Totals 91 2184.0 4.41384 4.28895 0.1249 130046.4 135.401 ,318 0.0120 99.2% 36.8
BHV-5 on stream % 99.1% BHV-5 Total Volume: 4.77E+06
Week Filter Start Stop Stop Start Total Total Loading, Per Cent
# Nu.m~r Dale Deter Gross· Tare Net Time Time Time Liters mslln3 OnStraom SCFM
1 8399050 31-Dec-12 07-Jan-13 4.4244 4.2908 0.1 336 53255.4 53090.0 9922.8 10,255,858 0.0130 96.4% 36.5
2 8399042 07-Jan-13 14-Jan-13 4.4676 4.3504 0.1172 53417.0 53255.4 9699.0 10,161,869 0.0115 96.2% 37.0
3 8399039 14-Jan-13 21-Jan-13 4.4075 4.3501 0.0574 53588.6 53417.0 10293.0 10,784,216 0.0053 102.1% 37.0
4 8399030 21-Jan-13 28-Jan-13 4.4018 4.2877 0.1141 53752.3 53588.6 9822.0 10,290,739 0.0111 97.4% 37.0
5 8399024 28-Jan-13 04-Feb-13 4,3675 4.3204 0.0671 53920.8 53752.3 10113.6 10,596,255 0.0063 100.3% 37.0
6 8399020 04-Feb-13 11-Feb-13 4.5321 4.3339 0.1982 54086.3 53920.8 9928.8 10,402,635 o.o1g1 98.5% 37.0
7 8399012 11-Feb-13 18-Feb-13 4_3284 4_2411 0.0873 54254.2 54086.3 10077 0 10,529,373 0.0083 100.0% 36.9
a 8399009 18-Feb-13 25-Feb-13 4.3792 4.2682 01110 54425.0 54254.2 10247.4 10,707,423 0.0104 101.7% 36.9
9 8399200 25-Feb-13 04-Mar-13 4.2846 4.2495 0.0351 54588.2 54425.0 9789.0 10,228,444 0.0034 97.1% 36.9
10 8399195 04-Mar-13 11 -Mar-13 4.4278 4.2825 0.1453 54751.5 54588.2 9796.8 10,153,370 0.0143 97.2% 36,6
11 8399188 11-Mar-13 18-Mar-13 4.3813 4.1879 0.1934 54917.0 54751.5 9912 4 10,237,655 0.0189 98.5% 36.4
12 8399183 18-Mar-13 25-Mar-13 4.5012 4.2614 0.2398 55084.5 54917.0 10048.8 10,357,632 0.0232 99.7% 36.4
13 8399179 25-Mar-13 01-Apr-13 4.4419 4.1991 0.2428 55254.4 55084.5 10193.4 10,506,676 0.0231 101.1% 36.4
Totals 91 2184.0 4.41272 4.27869 0.1340 129864 135,212,145 0.0129 9~1:,"/otp ~1 olfd?
Period: December 31 , 2013 through April 1, 2013 (1st Quarter 2013)
BHV-6 on .stream%
Week Filter Slart
If Numbet Elllle
1 8399051 31-Dec-12
2 8399041 07-Jan-13
3 8399040 14-Jan-13
4 8399029 21-Jan-13
5 6399023 28-Jan-13
6 8399021 04-Feb-13
7 6399011 11-Feb-13
8 8399010 18-Feb-13
9 8399199 25-Feb-13
10 8399194 04-Mar-13
11 8399187 11-Mar-13
12 8399184 18-Mar-13
13 8399180 25-Mar-13
Totals 91
ALL BHV on stream %
Week
# Blanks
Start
Date
1 8399046 31-0ec-12
2 6399035 07-Jan-13
3 8399034 14-Jan-13
4 8399028 21-Jan-13
5 8399022 28-Jan-13
6 8399016 04-Feb-13
7 8399005 11-Feb-13
8 8399004 18-Feb-13
9 8399193 25-Feb-13
10 8399192 04-Mar-13
11 8399186 11-Mar-13
12 6399175 18-Mar-13
13 8399174 25-Mar-13
Totals 91
99.1%
Stop
Dale
07-Jan-13
14-Jan-13
21-Jan-13
28-Jan-13
04-Feb-13
11-Feb-13
18-Feb-13
25-Feb-13
04-Mar-13
11-Mar-13
18-Mar-13
25-Mar-13
01-Apr-13
2184.0
99.4%
Stop
Date
07-Jan-13
14-Jan-13
21-Jan-13
28-Jan-13
04-Feb-13
11-Feb-13
18-Feb-13
25-Feb-13
04-Mar-13
11-Mar-13
18-Mar-13
25-Mar-13
01-Aor-13
2184.0
G•o5S
4.4531
4 4487
4.4402
4.4359
4.3647
4.5150
4.3833
4.4273
4.2654
4.4292
4.3975
4.4128
4.4214
4.41496
Net
4.3316
4.3472
4,3571
4.3304
4.3123
4.2918
4.3123
4.3426
4.2310
4.2037
4.2346
4.2117
4.2269
4.2872
Stop
TiliO Net lima
4.3334 0.1197 1656.3
4.3402 0.1085 1817.9
4.3378 0.1024 1989.5
4.3007 0.1352 2153.2
4.3273 0 0374 2321.4
4.3362 0.1786 2487.2
4.3068 0.0765 2655.4
4.3171 0.1102 2826.0
4.2353 0.0301 2989.2
4.2869 0.1423 3151 6
4.2277 0.1698 3317.2
4.2544 0.1584 3484.7
4.2242 0.1972 3654.7
4.29446 0.1205
Page2
BHV-6 Total Volume: 4.77E+06
Start Total Total Loading, Per Cent
nmo Tlmo Llb:mv maf"'3 On Stroarn SCFM
1491.0 9915.6 10,248,416 0.0117 96.4% 36 5
1656.3 9693.0 10,155,582 0.0107 96.2% 37.0
1817.9 !0297.2 10,788,617 0.0095 102.2% 37.0
1989.5 9820 8 10,269,481 0.0131 97.4% 37.0
2153.2 10095.0 10,576,767 0.0035 100.1% 37.0
2321.4 9948.0 10,422,752 0.0172 98.7% no
2487.2 IOOR9 6 10,542,539 0.0073 100.1% 36.9
2655.4 10239.0 10,698,646 0,0103 101.6% 36.9
2826.0 9793.2 10,232,833 0.0029 97.2% 36 9
2969.2 9740.4 10,094,917 0.0141 96.6% 36.6
3151.6 9937.2 10,242,602 0.0166 98.6% 36,4
3317.2 10049 4 10,358,251 0.0153 99.7% 36.4
3484.7 10198.2 10,511,624 0.0188 101.2% 36.4
129816.6 135.163,027 0.0116 99.1% 36.8
Page 22 of22
IJHV-1 on stream%
Week Filter
II Number
(, .,
X
I)
Ill
II
I?
1.'~ -
K199173
83'<9163
Xj'J<JI60
x:w<J 151
8399 I •IX
R399 I ~3
x:;9Q 132
X3'1913 I
KJ99120
K3'19118
8399113
8399102
K-100897
Toial<
Start
Date
1-Apr-13
08-Apr-l.l
15-Apr-13
1:2·Apr-13
2'1-Apr-13
06-May-IJ
13-May-13
20-May-13
28-May-13
03-Jun-13
11-Jun-13
17-Jun-13
2S·Jun-13
92
Ill IV-2 on stream %
Week filter
II N b um er
1 8399172
2 8399164
3 8399159
~ 8399152
5 8399147
6 8399142
7 8399133
B 8399130
9 8399121
10 8399117
11 8399112
1? 8399103
13 8400898
" Totals ...
Start
D ate
01-Apr-13
08-Apr-13
15-Apr-13
22-Apr-13
29-Apr-13
06-May-13
13-May-13
20-May-13
28-May-13
03-Jun-13
11-Jun-13
17-Jun-13
25-Jun-13
92
Bl IV-4 on stream %
Week Filter Start
# Number Date -1 6399171 01-Apr-13
? 8399165 08-Apr-13
3 8399158 15-Apr-13
~ 6399153 22-Apr-13
5 8399146 29-Apr-13
6 8399141 06-May-13
( 6399134 13-May-13
B 8399129 20-May-13
9 8399122 28-May-13
10 8399116 03-Jun-13
11 8399111 11-Jun-13
12 8399104 17-Jun-13
13 11-400899 25-Jun-13
Totals 92
BHV-5 on stream %
Week Filter Start
II NUmbeo-DB Iii
1 11399170 01·Apr·13
? 8399166 08-Apr-13
3 8399157 15,Apr-13 , 8399154 22-Apr-13
!) 8399145 29-Apr-13
6 8399140 06-May-13
7 8399135 13-May-13
8 8399128 20-May-13
9 8399123 28·May-13
10 8399115 03-Jun-13
11 8399110 11-Jun-13
12 8399105 17-Jun-13
13 8400900 25-Jun-13
Totals 92 -
98.1%
Stop
D&to
8-Apr-13
15-Apr-13
22-Apr-I 3
29-Apr-13
6-May-13
13-May-IJ
20-May-13
2&-May-13
3-Jun-13
11-Jun-13
I 7-Jun-I 3
24-Jun-13
2-Jul-13
2208.0
1010%
Slop
0 ate
08-Apr-13
15-Apr-13
22-Apr-13
29-Apr-13
06-May-13
13-May-13
20-May-13
28-May-13
03-Jun-13
11-Jun-13
17-Jun-13
24-Jun-13
02-Jul-13
2208 0
100.5%
Stop
Dale
08-Apr-13
15-Apr-13
22-Apr-13
29-Apr-13
06-May-13
13-May-13
20-May-13
28-May-13
03-Jun-13
11-Jun-13
17-Jun-13
24-Jun-13
02-Jul-13
2208.0
100.7%
Stop
Oale
08-Apr-13
15-Apr-13
22-Apr-13
29-Apr-13
06-May-13
13-May-13
20-May-13
28-May-13
03-Jun-13
11-Jun-13
17-Jun-13
24-Jun-13
02-Jul-13
2208.0
Gr s OS
·1 3557
4 5201
4.8340
•14685
4 662 I
4.3775
4.5700
4.9232
4.5432
4.6498
4.7268
4.5904
4 8052
4.617•123
ross
4.4576
4.9915
5 0026
4.4944
4 6742
4.5160
5.1152
5.0585
4.5511
4.7082
4.7178
4.7945
4.7364
4.755231
.Gross
4.3658
4.7036
5 2701
4.4340
4.4350
4,3896
4.4202
4.5211
4 4137
4 5180
4 4579
4.4421
4.5767
4.534446
Gross
. 4.4034
5.0346
5.3802
4,6587
4.7182
4.4511
4.6365
5.0990
4.4931
4.7053
4.5891
4.5609
4.7655
4.730431
Tar e Nl e
4.~0·10 (U517
•1 1'138 0 3263
·l.~I'N ()(,J.i(J
4 1158 () ~227
•U763 0 3858
4 2031 0.174•1
4 3142 0.2558
•1.3003 0.6229
4.2573 0.2859
4.3306 0.3192
4 3079 0.4189
4.3044 0.2860
4.3•11 K 0 •1634
, 269146 () 3483
T . -are N et
4.2059 0 2517
4.2340 0 7575
4.2067 0 7959
4.2521 0 2423
4.2535 0.4207
4.2985 0.2175
4.2957 0.8195
4.2618 0.7967
4.3027 0.2484
4.2974 0 4108
4.3377 0 3801
4.3123 0.4822
4 2880 0.4484
4.27279 0.4824
Tare Net
4.2362 01296
4.2419 0.4617
4.2332 1.0369
4.3260 0 1080
4.2189 0.2161
4.3193 0.0703
4.3033 0.1169
4 2892 0 2319
4.2973 0 1164
4.3177 0 2003
4.3268 0 1311
4,2963 0.1458
4.3142 0.2625
4.28618 0 2483
Taro Net
4 2024 0.2010
4.1549 0 8797
4.2561 1 1241
4.2662 0 3935
4.2724 0.4458
4 2880 0.1631
4 3247 0.3118
4.2966 0.8024
4 2760 0.2171
4.3336 0.3717
4.2735 0.3156
4.2924 0.2685
4.3255 0.4400
4.27395 0.4565
Stop
if rmo
461255
.J(J:l9•1 8
•IMC>JU
46630.6
46798.'1
16965.5
47134.'1
·17324 7
•17466.0
•17648.2
477&5.0
47911.6
·18101 8
Slop
T erne
56327.7
56497,0
56665.2
56832.5
57000.6
57167 2
57336.7
57526.9
57672.5
57862.9
58006.8
58178.0
58367.8
Stop
Time
31617.9
31788 2
31955.4
32123.8
32292.3
32453.8
32622 2
32812.4
32956.4
33153.1
33292.2
33463.0
33646 8
Stop
J Tlrne
55420.2
55590.5
55757.7
55926.0
56094.0
56260.7
56429.0
56619.3
56763.4
56959.6
57-099.2
57270.0
57453.8
BHV-1
Start
Tl me
•15'JS9 '!
•1612:1:1
•16294 H
·IM63JJ
·16630.6
•16791! 4
46965.5
·171 J.l •I
·1732,1.7
·17·166 0
476-18 . .?.
47785.0
,'17'111 6
BHV-2
Start
Time
56162,3
56327.7
56497.0
56665 2
56832.5
57000.6
57167.2
57336.7
57526.9
57672.5
57862.9
58006 8
58178 0
BHV-4
Start
Tlme
31452.0
31617.9
31788 2
31955.4
32123.8
32292 3
32453.6
32622.2
32812 4
32956.4
33153.1
33292.2
33463.0
BHV-5
Start
Time
55254.4
55<120.2
55590.5
55757 7
55926.0
56094,0
56260.7
56429 0
56619 3
56763 4
56959.6
57099.2
57270.0
Total
T rme
LJ936 6
101 5(, 2
101l<J3.~
10056.0
10065 (,
I(XIH:l
10138.8
11414 ·I
K4~04
10930.2
8108 6
75'17.2
1140'1.6
1~85 I I
Total
T lmc
'J921 (I
10 I ;c, J.
100'!50
IOOJ5J)
10086 6
9996 6
10170.0
11·11 ~.}
~738.'1
I J.i2.-lll
~631 N
1(127!1 ~
113HXJI
132327.6
Total
Time
99~5.2
1011&.0
HHH?..6
10101.6
10115.'1
%MM,7.
1010! .. ~
I 1413.1
M63<J •I
117'111 I)
~35 I .-1
10/-17!1
llU26.X
131691
Total
Time
I)IJ.I~ i')
1021'1.~
IOOJ" (,
100'17·1
f()iJ?NI!
100115.6
W0116.H
11·118.6
MM-1 8
I I 77~.0
8375.'1
10248.0
I t031.0
131968.2
Total Volume·
Total
L rters
1o.no.121
I 0.6•10,8X8
10.57-I.XXI
10,535,')()(>
I 0.5·'15,964
10,502,588
10,593,948
11,926,Kil
K,861 ,099
11.328,022
8,460,877
7,&30,687
11,7(,0,7.54
13J,K3?.,046
Total Volume:
Total
Liters
10,253,998
10,640.888
10,576.767
10.513,904
10,567,966
10,473,671
10,626,548
11 ,925.557
9,130,681
11,839,795
8,898,114
10,586,455
11 }37,990
137,772.334
4.73E+06
Loading, Per Cent
mufm3 0 s n tream
0 014R {)K 6~~;,
0 0307 IOO.H%
IJ.fliXI JOCJ.I c~{.
().()111 YY.X~.~Ju
0 036(, 99 9'}';,
00166 99A'~·o
0.0241 11!0.6%
0.052~ 99 I ~.1-.
0.0323 9R.2'.~~.
0 02~2 94 '!%
0.0495 95.0%
0.0365 75.'11Yr..
0.039·1 113_'!01..
11.0339 9KI'!~)
4.87E+06
Loading, Per Cent
mglmJ On Stroam
0.0245 98.4%
0.0712 100.8%
0 0752 1001%
0.0230 99.6%
0.0398 100.1%
0.0208 99.2%
0.0771 100.9%
0.0668 99.1%
0 0272 1011%
0 0347 99.2%
0.0427 99.9%
0.0455 101.9%
0.0382 113.0%
0.0451 101.0%
Total Volume: 4.84E+06
Total Loading, Per Cent
Liters mg/m3 On Stream
10,289,345 0.0126 98 8%
10,705,637 0.0431 1014%
10,511,389 0.0986 99,5%
10,563,682 0_0102 100.2%
10,598,141 0.0204 100.4%
10,150,553 0.0069 961%
10,556.331 0.0111 100 2%
11,925,557 0 0194 99.1%
9,027,237 0.0129 100.0%
12,228,443 0 0164 102.4%
8,608,066 0.0152 96 7%
10,562,336 I' 0.0138 1017%
11.365,689 0 0231 109.4%
137,112.407 I 0 0234 100.4%
Total Volume: 4.85E+06
Total Loading, Per Cent
lllers mgln\3 Or> Stroam
10,281,904 0.0195 98 7%
10,706,894 0.0622 101.4%
10.511,389 0.1069 99.5%
10,579,282 0.0372 100.2%
10,559,794 0.0422 1000%
10,483,101 0.0156 99.3%
10,550,062 0.0296 100,2%
11,931,200 0.0673 99.1%
9,032,879 0.0240 100.1%
12,200,461 0.0305 102 2%
6,632,803 0.0366 96.9%
10,562,954 0.0254 1017%
11.370.018 0.0387 109.4%
137,402,741 0.0427 100,7%
Page 1
scrM
)(l 5
J'/ ll
.<7.0
.l'lll
.n.o
:17 0
J6lJ
36.9
36 'I
J(, (,
J(, ·I
36. (
36.1
31>.X
SCFM
:'6.~
371l
3"/ [t
J'/,11
~7 (I
3711
31> 'I
36 ')
36 ()
36 6
31> •I
36 I
36 .j
)(>.~
S~CFM
36 5
.17 (i
3'1 IJ
J'/11
:17.11
J7 II
J6lJ
3(, l)
J61J
16 r,
36. I
31•.'1
36 d
3C>.X
St;I'M
~(1,.'\
3711
J"/JI
.17 (I
37ll
37 (I
J(, 9
36 9
J(, I)
3(,,(,
36A
.16 II
36 ·I
.Ill H
Page 21 of 22
-
.
Period: April1, 2013 through, July 2, 2013 (2nd Quarter 2013)
Week
II
1
/
3
4
s
6
I
8
9
10
11
1?
13
Week
I!HV-6 on stream%
r--;tter Start
Number DatQ
8399169 01-Apr-13
8399167 08-Apr-13
8399155 15-Apr-13
8399156 22-Apr-13
8399144 29-Apr-13
8399139 06-May-13
8399136 13-May-13
8399127 20-May-13
8399124 26-May-13
8399114 03-Jun-13
8399109 11-Jun-13
8399106 17-Jun-13
8399101 25-Jun-13
Totals 92
ALL BHV on s1ream %
II lllanks
Start
Date
1
?
3 ..,
~
6
7
8
9
10
11
1?
13 -
.8:199182.
8399161
8399150
8399149
8399138
8399137
8399126
8399125
8399119
8399108
8399107
8400896
8400890
lotals
01-Apr-13
08-Apr-13
15-Apr-13
22-Apr-13
29-Apr-13
06-May-13
13-May-13
20-May-13
28-May-13
03-Jun-13
11-Jun-13
17-Jun-13
25-Jun-13
92.
100.7%
Stop
Oale
08-Apr-13
15-Apr-13
22-Apr-13
29-Apr-13
06-May-13
13-May-13
20-May-13
28-May-13
03-Jun-13
11-Jun-13
17-Jun-13
24-Jun-13
02-Jul-13
2208_0
100.2%
Stop
Date
08-Apr-13
15-Apr-13
22-Apr-13
29-Apr-13
06-May-13
13-May-13
20-May-13
28-May-13
03-Jun-13
11-Jun-13
17-Jun-13
24-Jun-13
02-Jul-13
2208.0
Gross
4.4957
4.9099
5.3214
4.7086
4 9200
4.3896
4 6910
4.7378
4.5071
44970
4.6937
4 5672
4 6983
4_704408
Nel
4 1959
4,2404
4.2315
4.2295
4.3162
4.3027
4.2898
4.2861
4.3206
4.3305
4.3047
4.3454
4.3313
4.2865
Stop
Tam et Time
4 1864 0 3093 3820.5
4.2307 0,6792 3990.8
4.2280 1 0934 4158.0
4 1830 0.5256 4326.1
4.2512 0.6688 4494.6
4.2769 0.1127 4661.1
4.3180 0.3730 4829.5
4.2584 0.4794 5019.7
4.2696 0 2375 5163,7
4.3162 0.1808 5360.3
4.3278 0.3659 5499.5
4.3129 0 2743 5670.3
4.2543 0 4440 5654.1
4.26257 0.4418
Paga ;>
BHV-6 Total Volume: 4.85E+06
Start Tolal Tolal loading. Per Cent
Time Timo Loters mg}m3 On Stream SCI M
3654 7 'J950 ,j 10,284,384 0.0301 98 7% :,(,_.' I 3820 5 10?.1'!,:< 10,706,894 0 0634 101.4% :n.11
3990 8 I(IOJ3 H 10,512,646 01040 99,5% 3"l \}
4158 0 10ll8J.6 10,564,823 0.0498 100.0% ]'/,0
4326 1 1010'!.-1 10,591,854 0.0631 100.3% 371l
4494 6 91)KK R 10,465,499 0.0108 99.1% 37 0
4661 1 lUl U~.'-10.561,974 0.0353 100.3% 36'>
4829 5 II 107.S 11 ,919.915 0.0402 99.0% .}(ll)
5019.7 SMI ) 9,029,118 0.0263 100.0% J6_()
5163 7 1179'>.0 12.228,4<13 0.0148 1024% 36.li
5360.3 ~J51 •I 8.608,066 0,0425 96.7% ]6 -I
5499.5 11!:<'16.~ 10,561,717 0.0260 101.7% 36 -I
5670 3 11029.~ 11,368,163 0.0391 109.4% 36 ~
131968 8 137.403.497 0.0419 100.7% J6 X
Page 22 of22
ATTACHMENTE
ENVIRONMENTAL GAMMA GRAPHS AND SUPPORTING DATA
I White Mesa Mill Ambient Gamma Levels Over Time I
50.00~-------------------------------------------------------------------------------------------------------------------.
45.00 +---------------------------------------------------------------------------------------------~~------------------------~
4o.oo I ;&
35.00 ~ I I • I I -. I
30.00
.....
Q)
t:: 25.00 en :::::!
0" --E Q)
II: 20.00
E
15.00
10.00 I I H-----------------------------------------1:-j
5.oo ~-llllll-l·liiillmR-,..._I~Ft:A:: I W. Tl:::a r I W -• I 11+-±-1 I :1.: I I _ 8 I a.l I 41::::1--1-H-+'l!M!t
0.00 IIRI'lt~i= ~
30.-sep..81 05-Jul-83 04-APr-as 03-Feb-87 11-0ct-88 16-.Jul-9o 10-A.Pr-92 13-Jan-94 16-0ct-95 8-Juf-97 13-A.Pr-99 20-Feb-o1 1S..oct-o2 9-Jul-04 10-A.Pr-o 31-Dec-o 2-0ct-o9 Vi!Hrr12 1\.tf:. 30-seP-81 6 7 SA. MILL
Background (BHV-3) subtracted from BHV-1, BHV-2, BHV-4, BHV-5, and BHV-·6
I -BHV-1 -+-BHV-2 -BHV-3 -BHV-4 -BHV-5 -BHV-6 I
I White Mesa Mill Ambient Gamma Levels Over Time BHV-1]
50.00
45.00
40.00
35.00
30.00
.....
Q) t:: Ill 25.00 :::J .!! E Q) a: 20.00 E
15.00
10.00 ~·---------------------------------------------------------------------ir------------------------------------------~
5.oo ~--A-1· e I •
o.oo ~ ¥ :i 8!1 ... :: :. ~ ee·~, ~-~' m t.-MM..~-~ 4li ~ t aJOsa?A 1 r · .M
~R ~ ~0 •o -0 ~R &Oc ~0 ~N ~0 -0 &Oc ~0 -0 ~ ~ w"<>ep-81 Oct-83 Cf-85 Cf-87 Cf-89 ~eP·9t t-93 Cf-95 D\f-97 ct-99 ct-o1 t-o3 Cf-05 ct-07 "'-T•09 "C1" R,q DIA,1"ION
Background (BHV-3) Subtracted from BHV-1
-+-BHV-1
I White Mesa Mill Ambient Gamma Levels Over Time BHV-21
50.00~------------------------------------------------------------------------------------------------------,
45.00 +-------------------------------------------------------------------------------------------------------~
40.00 +-------------------------------------------------------------------------------------------------------~
35.00 +-------------------------------------------------------------------------------------------------------~
30.00 ......
Q)
t::
ell
:::l 0" 25.00 -E
Q) a:
E 20.00
15.00 I
10.00 I
5.oo I Ji' IH+e • • A 1f I
o.oo IM·Aif!~~ ... :=.i-.~~-j .·¥.-.~iiUiiW· .. ~~·e.eH•,~~wn L'lt.-. .. ~w.· .... I/Jt .•.. .,.,~
a(J_co. 03.0· 01.0 09-0 3o.0 3o.8 8-0ct 16-o 10.A• 12.0 24-o 3-0ct 11.0 3o.0 2-0ct DtRr.-c -oeP-81 ct-83 ct-Bs ct-87 ct-89 ep.91 -93 ct-95 •vov.97 ct-99 ct-o1 -03 ct-os ct-07 -09 "'' i R.4
D!AiJoN
Background (BHV-3) Subtracted from BHV-2
I -+-BHV-2 I
50.00
45.00
40.00
35.00
30.00 ......
Q) t: cu :::::! c-25.00 --E Q) a:
E 20.00
15.00
10.00
5.00
0.00
30-seP-81 03-0ct-83 07-oct-Bs 09-0ct-87 30-0ct-89
[White Mesa Mill Ambient Gamma Levels Over Time BHV-3 1
3o-seP-91 B-oct-93
Background (BHV-3)
16-0ct-95 10-fVov-97 12-0ct-99 24-0ct-01
-+-BHV-3
3-0ct-03 17-0ct-os 30-oct-o7 2-0ct-o9 DIRt:c; RAo,Ai!oiV
I White Mesa Mill Ambient Gamma Levels Over Time BHV-4j
50.00~------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------,
45.00 +-----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------__,
40.00 +-----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------~
35.00 +---------------------------------------------------------------------------------------------------------------------------------~
30.00
......
Q)
t:: 25.00 ro ::J .!:! E Q) a: 20.00
E
15.00
10.00 +------+t-------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------~
5.00 I '!!I' I .6o I ff-I
0.00 ~ " , -' . i @I 1 ••• 1 --g.~ . .,_. i!·~-. ''H!!H
3o.s~P-81 03-ocr-s3 07-0ct-ss 09-0ct-s7
30-0ct-89 30-sep.91 B-oct-93 1B-oct-9s 10-Nov-97 12-0ct-99 24-0ct-01 3-0ct-03 17-oct-os 3o.oct-07 2-0ct-o9 DIRE::cl %fAlloN
Background (BHV-3) Subtracted from BHV-4
r -~ I
.....
Q)
t ctl
::J 0" -E
Q) a:
E
I White Mesa Mill Ambient Gamma Levels Over Time BHV-sl
50.00 ~----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------~
45.00 +-----------------------------------------------------------------------------------------------~
40.00 +---------------------------------------------------------------------------------------------------~
35.00 +---------------------------------------------------------------------------------------------------~
30.00
25.00
20.00
15.00 +---------------------------------------------------------------------------------------------------------~
10.00 +------------------------------------------------------------@~------------------------------------~
5.00 I I 1---H!IJ -... I:IBA F\;. .... ..,. lanA I I • -w I I 1: I I :Jr.: I I 'Jll' 1-I I I 1 \ I
o.oo F@·t!IJ··,·:-'j·,·,-.-:,·,·,·,·,·,·;:w·•··········· , , , ·.-,·,·@t·8 ·tt ,·,·,·:.-.·:w·:• ,._.,.,·,·,·•· •~···················•·····•'(• ..•. ,.,,,,,.,,. , , _.,.,.,._, ••. ...,. ,·,·:c:·,x.·.·.·,-.·.z .... ,.,
30-sep.81 03-0ct-83 07-0ct-es 09-0ct-87 30-0ct-89 30-Sep-91 B-Oct-93 16-0ct-95 10-Nov-97 12-0ct-99 24-0ct-01 3-0ct-03 17-0ct-os 30-0ct-07 2-0ct-09 Dlf?f2cr !'?A
D!41JoN
Background (BHV-3) Subtracted from BHV-5
I ....--BHV-5 I
I White Mesa Mill Ambient Gamma Levels Over Time BHV-61
50.00
45.00
40.00
35.00
30.00
"-Q) t:: co 25.00 :::::1
0" --E
Q) a: 20.00
E
15.00
10.00
5.00
0.00 ----1~ _,A _.[\,.._ .
_,' _,' .. I . '' ... ~~ -~ ~~-
30-seP-81 03-0ct-a3 07-0ct-as 09-oct-a7 3o.Oct-a9 3o.seP-91 B-oct-93 1&.oct-9s 1o... 12.0 24-o 3-o •vo".97 ct-99 ct-o1 ct-03 17-0ct 30..n.t 2-0ct-" -os --c '()7 -v9 Dl~t:cr RAo,A /JoN
Background (BHV-3) Subtracted from BHV-6
--+-BHV-6
Badge
Number
Control
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
45
46
47
50
51
52
53
64
White Mesa Mill First Quarter 2013 Environmental Spherical Gamma Monitor Results
Location
Administration Vault
V205 Control Room
BHV-6
Ore Stor. -Barrel Area
Vanadium Precip.Area
Yellocake Drying Area
Leach
SAG Mill Control Room
Yellowcake Precip.
Central Control Room
Trammel Screen (ore pad)
North East Corner Ore Pad
Met. Lab
Filter Press Room
BHV-1
BHV-2
BHV-3
BHV-4
BHV-5
SAG Mill
Tails
CCD
North SX
Administration Building
Admin Parking Lot
Yellowcake Packaging
Yellowcake Storage
Bucking Room
Mill Lunch Room
South SX
Mtce. Super.'s Office
Ore Feed Grizzly
Scalehouse
Sample Plant (OBS)
Front Gate
AF-Barrel Dump Station
AF Circuit -South
AF Circuit-North
Pinenut Travel Way
North Control # 1
North Control# 2
CaF2 Barrel Dump Station -
Operator Station
KF Barrel Dump Station
Date Issued
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/3112012
12/31/2012
12/3112012
12/31/2012
12/3112012
12/31/2012
12/31/2012
12/31/2012
12/3112012
12/31/2012
12/3112012
12/3112012
12/3112012
12/31/2012
12/3112012
12/31/2012
12/31/2012
12/31/2012
12/31/2012
12/3112012
12/3112012
12/3112012
12/31/2012
12/31/2012
12/31/2012
Total Days
Badge at
Date Returned WMM
3/28/2013 87
3/28/2013
3/28/2013
3/28/2013
3/2812013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/2812013
3/28/2013
3/28/2013
3/28/2013
3/2812013
3/28/2013
3128/2013
3/28/2013
3/28/2013
3/2812013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
312812013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/2812013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
87
Mean
Ambient
Dose
Equivalent
31.9
45.9
25.7
171
83.4
226.9
260.8
181.6
80.4
131.1
217.7
57.3
159.3
32
27.8
27.2
27.5
30
331.5
48.9
68.4
66.6
35.9
75.4
1512.2
500.6
118.4
50.1
92.3
41.3
384.8
213.7
216.4
179.5
268.6
31.3
87.5
29.9
33.9
28.9
317.5
264.3
mRem/ mRem/
hour Day
0.02 0.367
0.02
0.01
0.08
0.04
0.11
0.00
0.12
0.09
0.04
0.06
0.10
0.03
0.08
0.02
0.01
O.Ql
0.01
0.01
0.16
0.02
0.03
0.03
0.02
0.04
0.72
0.24
0.06
0.02
0.04
0.02
0.18
0.10
0.10
0.09
0.13
0.01
0.04
0.01
0.02
0.01
0.15
0.13
0.528
0.295
1.966
0.959
2.608
0.000
2.998
2.087
0.924
1.507
2.502
0.659
1.831
0.368
0.320
0.313
0.316
0.345
3.810
0.562
0.786
0.766
0.413
0.867
17.382
5.754
1.361
0.576
1.061
0.475
4.423
2.456
2.487
2.063
3.087
0.360
1.006
0.344
0.390
0.332
3.649
3.038
mRem/
Week
2.57
3.69
2.07
13.76
6.71
18.26
0.00
20.98
14.61
6.47
10.55
17.52
4.61
12.82
2.57
2.24
2.19
2.21
2.41
26.67
3.93
5.50
5.36
2.89
6.07
121.67
40.28
9.53
4.03
7.43
3.32
30.96
17.19
17.41
14.44
21.61
2.52
7.04
2.41
2.73
2.33
25.55
21.27
White Mesa Mill Second Quarter 2013 Environmental Spherical Gamma Monitor Results
Badge
Number Location
Control Administration Vault
1 V205 Control Room
2 BHV-6
3 Ore Stor. -Barrel Area
4 Vanadium Precip. Area
5 Yellowcake Drying Area
6 Leach
7 SAG Mill Control Room
8 Yellowcake Precip.
9 Central Control Room
10 Trommel Screen (ore pad)
11 North East Corner Ore Pad
12 Met. Lab
13 Filter Press Room
14 BHV-1
15 BHV-2
16 BHV-3
17 BHV-4
18 BHV-5
19 SAG Mill
20 Tails
21 CCD
22 North SX
23 Administration Building
24 Admin Parking Lot
25 Yellowcake Packaging
26 Yellowcake Storage
27 Bucking Room
28 Mill Lunch Room
29 South SX
30 Maint. Super.'s Office
31 Ore Feed Grizzly
32 Scalehouse
33 Sample Plant (OBS)
34 Front Gate
45 AF -Barrel Dump Station
46 AF Circuit-South
47 AF Circuit -North
51 North Control# 1
52 North Control # 2
CaF2 Barrel Dump Station -
53 Operator Station
64 KF Barrel Dump Station
Date Issued
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
3/28/2013
Date Returned
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
6/26/2013
7/11/2013
Total Days
Badge at
WMM
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
105
Mean
Ambient
Dose mRem/
Equivalent hour
32 0.01
46.1 0.02
58 0.03
196.4 0.09
99.4 0.05
258.9 0.12
0.00
350.8 0.16
273.5 0.13
92.3 0.04
150.8 0.07
0.00
60 0.03
165.1 0.08
32.7 0.02
28.9 0.01
27.7 0.01
30.8 0.01
30.9 0.01
336 0.16
29.1 O.Ql
85.4 0.04
63.2 0.03
35 0.02
85.1 0.04
1600.1 0.74
694.6 0.32
129.5 0.06
50.3 0.02
114.1 0.05
46 0.02
277.7 0.13
212.8 0.10
210.8 0.10
210.4 0.10
536.3 0.25
72.3 0.03
148.6 0.07
36.3 0.02
30.8 0.01
338.4 0.16
239.3 0.09
mRem/
Day
0.356
0.512
0.644
2.182
1.104
2.877
0.000
3.898
3.039
1.026
1.676
0.000
0.667
1.834
0.363
0.321
0.308
0.342
0.343
3.733
0.323
0.949
0.702
0.389
0.946
17.779
7.718
1.439
0.559
1.268
0.511
3.086
2.364
2.342
2.338
5.959
0.803
1.651
0.403
0.342
3.760
2.279
mRem/
Week
2.49
3.59
4.51
15.28
7.73
20.14
0.00
27.28
21.27
7.18
11.73
0.00
4.67
12.84
2.54
2.25
2.15
2.40
2.40
26.13
2.26
6.64
4.92
2.72
6.62
124.45
54.02
10.07
3.91
8.87
3.58
21.60
16.55
16.40
16.36
41.71
5.62
11.56
2.82
2.40
26.32
15 .95
ATTACHMENT F
VEGETATION GRAPHS, DATA TABLE, LABORATORY RESULTS AND QAJQC
(Log Scale)
_.. _.. _..
0 0 0 0 0 0 0
0 0 0 0 0 0 0 m m m m m m m
I I I 6 I I I
0 0 0 0 0 0
CX> -...1 0> (11 ~ w 1\)
8/27/1981
8/27/1982
8/27/1983
8/27/1984
8/27/1985 ..
8/27/1986
8/27/1987 .
8/27/1988
8/27/1989 ::0 D)
I
8/27/1990 N N 0)
8/27/1991 0 0
8/27/1992 ::::J (')
CD
8/27/1993 . ::::J -...
8/27/1994 . D) -s·
f 8/27/1995 ::::J 0
z 8/27/1996 :r m < 8/27/1997 CD
T
cc
8/27/1998 CD -D) -z 8/27/1999 s· :E ::::J
8/27/2000 -c
f 8/27/2001 0 :::::::
(JJ 8/27/2002 ~
:E cc -8/27/2003
8/27/2004
8/27/2005
8/27/2006
8/27/2007
8/27/2008
8/27/2009 .
8/27/2010
8/27/2011
8/27/2012 •.
8/27/2013
(Log Scale)
_. _. _.
0 0 0 0 0 0 0
0 0 0 0 0 0 0 m m m m m m m I I I I I I I
0 0 0 0 0 0 0 CX> -...1 Ol (}1 ~ w I\)
8/27/1981
8/27/1982
8/27/1983
8/27/1984
8/27/1985
8/27/1986
8/27/1987
8/27/1988
"'tt 8/27/1989 C" I
8/27/1990
1\) ......
0
8/27/1991 0 0
8/27/1992 ::::s n CD
8/27/1993 ::::s -""'' 8/27/1994 D) -a·
t 8/27/1995 ::::s en
z 8/27/1996 ::::s m < 8/27/1997 CD cc
T 8/27/1998 CD -D) -z 8/27/1999 a· :E ::::s
8/27/2000 -c t 8/27/2001 0
::::::.::
U> 8/27/2002 " :E cc -8/27/2003 ..
8/27/2004 .
8/27/2005
8/27/2006
8/27/2007 "
8/27/2008 -
8/27/2009 .,
8/27/2010
8/27/2011
8/27/2012
8/27/2013 .
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WHITE MESA MILL
FORAGE RADIONUCLIDE DATA
NORTHEAST OF MILL
SAMPLED QTR. SAMPLED DATE
3rd '81 27-Aug-81
4th '81 20-0ct-81
2nd'82 15-Apr-82
3rd '82 01-Jul-82
4th '82 30-Nov-82
2nd '83 13-Apr-83
3rd '83 01-Jul-83
4th '83 30-Jan-84
2nd'84 28-Jun-84
4th '84 14-Nov-84
2nd '85 27-Mar-85
3rd '85 15-Jul-85
4th '85 09-0ct-85
2nd'86 24-Mar-86
3rd'86 10-Jul-86
4th '86 18-Dec-86
2nd'87 20-Apr-87
3rd '87 05-Jun-87
4th '87 22-Dec-87
2nd'88 19-Apr-88
3rd'88 28-Jul-88
2nd '89 07-Apr-89
3rd '89 06-Jun-89
4th '89 07-Nov-89
1st '90 17-Apr-90
2nd'90 20-Jun-90
3rd'90 17-0ct-90
1st '91 10-Apr-91
2nd'91 11-Jun-91
3rd '91 20-Nov-91
1st '92 22-Apr-92
2nd '92 10-Jun-92
3rd '92 10-Jun-92
1st '93 13-Apr-93
2nd '93 26-Jun-93
3rd '93 12-0ct-93
1st '94 11-May-94
2nd'94 19-Jui-94
3rd'94 28-Nov-94
lst'95 11-Apr-95
2nd '95 06-Jui-95
3rd '95 15-Nov-95
1st '96 23-Apr-96
2nd '96 * 31-Jul-96
3rd '96 14-Nov-96
1st '97 21-Apr-97
3rd '97 05-Sep-97
4th '97 20-Nov-97
1st '98 23-Mar-98
2nd '98 16-Jun-98
4th '98 05-Nov-98
2nd '99 15-Apr-99
3rd '99 07-Jul-99
4th '99 02-Dec-99
2nd '00 21-Apr-00
2nd'OO 22-Jun-00
Ra-226 Ra-226
VALUE (uCi/Kg) ERROR (uCI/Kg)
3.90E·04 l.OOE-05
1.40E-04 l.OOE-05
1.31E·04 1.30E-05
1.60E·04 l.OOE-05
2.67E-06 1.07E-06
9.36E-05 6.20E-06
1.12E-04 1.20E-05
1.09E-04 8.00E-06
3.47E-04 1.20E-05
5.61E-04 1.99E-04
1.05E·03 3.00E-05
8.20E-05 7.00E-06
1.15E·04 l.OOE-05
5.72E-04 2.10E-05
5.01E-04 1.30E-05
8.70E-04 5.00E-05
5.90E-04 7.00E-05
1.60E-04 3.00E-05
2.10E-04 4.00E-05
4.50E-04 7.00E-05
3.20E-05 2.20E-05
5.60E-04 4.00E-05
1.50E-04 2.00E-05
6.00E-04 5.00E-05
2.60E-04 3.00E-05
1.80E-04 2.00E-05
1.60E-04 2.00E-05
1.20E-04 2.00E-05
9.10E-05 1.60E-05
4.50E-04 4.00E-05
3.60E-05 1.00E-05
1.00E-05 7.00E-06
7.90E-05 3.50E-05
3.70E-05 2.20E-05
3.00E-05 1.50E-05
6.60E-05 2.70E-05
l.BOE-04 4.00E-05
1.71E-05 1.20E-06
2.40E-04 1.50E-05
6.70E-05 5.40E-06
1.50E-05 1.50E-06
5.50E-05 S.OOE-06
5.20E-05 2.50E-06
3.00E-05 2.50E-06
l.lOE-05 4.70E-07
1.10E-05 4.30E-07
8.00E-06 1.20E-06
<9.10E-05 9.10E-05
1.80E-05 1.20E-06
5.70E-05 l.OOE-06
2.00E-04 3.00E-06
6.03E-05 1.40E-06
2.30E-05 l.OOE-06
1.50E-04 3.00E-06
1.20E-06 l.OOE-07
LLD Pb-210 Pb-210 LLD
uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (l.OE-06)
5.00E-08 l.lOE-03 1.00E-04 l.OOE-06
5.00E-08 6.80E-04 8.00E-05 l.OOE-06
l.OOE-06 4.90E-04 7.00E·05 8.00E-05
5.00E-08 8.00E·04 1.70E-04 l.OOE-07
l.OOE-06 1.08E-04 9.00E-06 l.OOE-05
8.00E-09 4.97E-04 9.30E-05 l.OOE-04
6.00E-06 1.84E-04 1.20E-05 1.00E-06
4.00E-06 7.80E-04 6.20E-05 6.00E-05
2.00E-09 3.75E-03 1.60E-04 4.00E-08
2.00E-07 7.82E-03 3.30E-04 7.00E-08
2.00E-06 3.22E-03 1.40E-04 2.00E-05
3.00E-06 7.70E-04 1.30E-04 2.00E-04
3.00E-06 5.10E-04 3.00E-05 2.00E-05
4.00E-06 2.49E-03 l.OOE-04 l.OOE-05
3.00E-06 1.57E-03 1.70E-03 2.00E-04
3.00E-06 6.80E-04 3.00E-05 3.00E-06
5.00E-08 1.50E-03 l.OOE-04 1.00E-06
5.00E-08 9.50E-04 4.00E-05 l.OOE-06
5.00E-08 1.70E-03 1.00E-04 l.OOE-06
5.00E-08 1.40E-03 l.OOE-04 l.OOE-06
5.00E-08 1.50E-04 4.40E-04 l.OOE-06
*** 1.10E-03 l.OOE-01 ***
*** 2.30E-04 2.00E-05 ***
7.00E-06 2.04E-03 7.00E-05 1.40E-05
4.00E-06 3.30E-04 2.00E-05 2.20E-05
5.00E-08 3.20E-04 2.00E-05 l.OOE-06
5.00E-08 3.30E-04 2.00E-05 l.OOE-06
5.00E-06 3.00E-04 2.00E-05 l.OOE-06
2.00E-07 1.90E-04 2.00E·05 2.00E-07
5.00E·08 1.09E-03 5.00E·05 l.OOE-06
2.00E-06 1.50E-04 2.00E-05 1.00E-05
2.00E-07 7.50E-05 2.00E-05 l.OOE-06
3.00E-06 7.10E-04 7.00E-05 2.00E-05
3.00E-06 2.80E-04 3.00E-05 2.00E-05
3.00E-06 4.30E-05 3.50E-05 2.00E-05
3.00E-06 5.30E-04 6.00E-05 2.00E-05
3.00E-05 4.40E-04 6.00E-05 2.00E-04
9.00E-08 3.00E-05 6.10E-06 4.45E-06
1.70E-07 1.70E-04 l.lOE-05 8.30E-07
1.60E-07 1.40E-04 1.30E-05 7.90E-07
1.50E-07 5.10E-05 4.50E-06 7.60E-07
1.80E-07 6.70E-05 l.OOE-05 8.80E-07
1.50E-07 3.20E-05 4.50E-06 1.80E-07
1.80E-07 1.40E-04 7.10E-06 9.30E-07
1.21E-07 4.10E-05 3.60E-06 6.10E-07
1.33E-07 2.10E-05 7.30E-07 6.66E-07
5.60E-07 1.40E-04 4.60E-06 l.lOE-07
9.10E-05 <4.50E·04 4.50E-04 4.50E-04
6.30E-08 4.00E-05 1.80E-06 3.20E-07
8.20E-08 8.70E-05 5.00E-06 4.10E-07
1.20E-07 3.00E-04 1.00E-05 6.00E-05
8.30E-08 1.40E-04 4.70E-06 4.20E-07
2.30E-07 2.10E-05 l.OOE-06 l.lOE-06
1.20E-07 1.60E-04 8.00E-06 5.90E-07
2.80E-07 1.60E-04 l.OOE-05 1.40E-06
4th '00 21-Dec-00 1.60E-06 l.lOE-06 3.70E-07 S.10E-OS S.OOE-06 1.90E-06
1st '01 30-Apr-01 l.OOE-06 l.OOE-07 2.40E-07 <1.2E-06 l.OOE-07 2.40E-07
2nd'01 14-Jun-01 2.30E-06 2.00E-07 9.90E-08 3.80E-06 2.00E-07 S.OOE-07
4th '01 17-Dec-01 9.10E-06 2.40E-06 1.20E-07 3.S7E-OS 2.97E-06 6.00E-07
1st '02 07-May-02 3.30E-OS 1.80E-06 7.60E-07 4.SOE-OS 2.61E-06 1.00E-OS
2nd'02 07-Jul-02 S.SSE-OS 2.81E-06 7.60E-07 S.31E-OS 3.90E-06 1.00E-OS
4th '02 1S-Dec-02 7.7SE-OS 3.60E-06 7.60E-07 1.29E-04 6.1SE-06 l.OOE-OS
1st '03 21-Mar-03 9.10E-06 1.30E-06 3.60E-07 1.13E-OS 1.61E-06 3.36E-06
2nd'03 10-Jun-03 2.SOE-OS 1.30E-06 3.60E-07 3.26E-06 2.00E-06 7.38E-08
4th '03 20-Nov-03 S.70E-OS 3.SOE-06 1.SOE-07 4.0SE-OS S.82E-06 8.30E-07
1st '04 08-Apr-04 9.38E-OS 3.70E-06 l.lOE-07 S.88E-OS 3.00E-06 S.SOE-07
2nd '04 12-Jun-04 S.63E-OS 3.40E-06 1.80E-07 6.42E-OS S.90E-06 9.00E-07
4th'04 30-Nov-04 8.41E-OS S.SOE-06 2.00E-08 2.48E-04 1.40E-OS 3.00E-07
1st 'OS 21-Apr-OS S.60E-OS 3.00E-06 1.40E-07 S.80E-OS 4.00E-06 6.90E-07
2nd 'OS 13-Jun-OS 9.10E-06 1.SOE-06 1.80E-07 1.10E-OS 1.20E-05 9.00E-07
4th'OS 10-Nov-OS 6.00E-OS 3.00E-06 l.lOE-10 1.70E-06 6.40E-07 S.SOE-10
1st '06 03-Apr-06 8.00E-OS S.OOE-06 S.OOE-08 3.40E-04 1.20E-OS l.OOE-06
2nd '06 16-Jun-06 4.10E-OS 3.10E-06 S.OOE-08 1.16E-04 6.10E-06 l.OOE-06
4th '06 28-Nov-06 1.17E-04 4.60E-06 1.90E-07 3.28E-04 9.SOE-06 9.SOE-07
1st '07 30-Mar-07 9.70E-OS 4.40E-06 1.90E-07 3.40E-04 8.70E-06 8.4-07
2nd'07 1-Jun-07 1.30E-OS 1.60E-06 1.90E-07 1.20E-04 6.60E-06 9.70E-07
4th '07 23-Nov-07 7.00E-OS 8.20E-06 2.00E-07 S.OOE-04 2.00E-OS 1.20E-06
1st '08 22-Apr-08 3.60E-06 3.00E-06 S.20E-07 2.30E-04 1.40E-OS l.OOE-06
2nd'08 18-Jun-08 3.20E-OS 3.20E-06 1.80E-06 6.90E-OS 3.SOE-OS S.SOE-OS
4th '08 12-Dec-08
1st '09 28-Apr-09 5.90E-04 1.3SE-OS l.SOE-06 3.40E-04 1.30E-OS 1.SOE-06
2nd'09 17-Jun-09 1.90E-OS 1.4SE-06 4.90E-07 3.60E-OS 1.10E-OS 1.80E-OS
4th '09 18-Dec-09 1.70E-04 S.90E-06 4.80E-04 1.20E-OS
1st '10 13-May-10 2.20E-04 7.20E-06 l.lOE-06 1.90E-04 1.90E-OS 2.90E-OS
2nd'10 18-Jun-10 6.SOE-OS 3.40E-06 7.60E-07 1.40E-04 1.90E-OS 2.90E-OS
4th'10 20-Dec-10 2.30E-OS 1.70E-06 5.20E-07 1.00E-05 1.SOE-06 2.30E-06
2nd '11 23-Jun-11 2.40E-07 1.40E-07 1.80E-07 <2.9E-06 1.70E-06 2.90E-06
2nd '12 11-Apr-12 4.40E-OS 1.90E-06 3.60E-07 2.10E-04 2.00E-06 l.OOE-06
3rd'12 11-Jun-12 2.20E-OS 8.40E-07 l.lOE-07 1.30E-04 7.60E-06 5.90E-06
4th '12 06-Nov-12 3.10E-OS 4.82E-07 4.63E-08 4.26E-04 3.72E-06 6.S2E-07
2nd '13 30-Apr-13 1.14E-04 1.74E-06 5.34E-07 2.6SE-04 4.41E-06 5.37E-06
3rd '13 20-Jun-13 8.91E-OS 2.16E-06 1.42E-06 1.42E-04 3.68E-06 6.17E-06
*2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period
WHITE MESA MILL
FORAGE RADIONUCLIDE DATA
NORTHWEST OF MILL
SAMPLED QTR. SAMPLED DATE
3rd '81 27-Aug-81
4th '81 20-0ct-81
2nd '82 15-Apr-82
3rd '82 01-Jui-82
4th '82 30-Nov-82
2nd'83 13-Apr-83
3rd '83 01-Jul-83
4th '83 30-Jan-84
2nd '84 28-Jun-84
4th '84 14-Nov-84
2nd'85 27-Mar-85
3rd '85 15-Jui-85
4th'85 09-0ct-85
2nd'86 24-Mar-86
3rd '86 10-Jul-86
4th '86 18-Dec-86
2nd'87 20-Apr-87
3rd '87 05-Jun-87
4th '87 22-Dec-87
2nd'88 19-Apr-88
3rd '88 28-Jul-88
2nd '89 07-Apr-89
3rd '89 06-Jun-89
4th '89 07-Nov-89
1st '90 17-Apr-90
2nd'90 20-Jun-90
3rd'90 17-0ct-90
1st '91 10-Apr-91
2nd'91 11-Jun-91
3rd '91 20-Nov-91
1st '92 22-Apr-92
2nd '92 10-Jun-92
3rd '92 10-Jun-92
1st '93 13-Apr-93
2nd '93 26-Jun-93
3rd'93 12-0ct-93
1st '94 11-May-94
2nd'94 19-Jul-94
3rd '94 28-Nov-94
1st '95 11-Apr-95
2nd'95 06-Jul-95
3rd '95 15-Nov-95
1st '96 23-Apr-96
2nd '96 * 31-Jui-96
3rd'96 14-Nov-96
1st'97 21-Apr-97
3rd '97 05-Sep-97
4th '97 20-Nov-97
1st '98 23-Mar-98
2nd'98 16-Jun-98
4th '98 05-Nov-98
2nd '99 15-Apr-99
3rd '99 07-Jul-99
4th '99 02-Dec-99
2nd'OO 21-Apr-00
Ra-226 Ra-226
VALUE (uCi/Kg) ERROR (uCi/Kg)
2.73E-03 5.00E-05
2.00E-04 1.00E-05
1.04E-04 9.00E-06
2.00E-05 l.OOE-05
2.36E-06 9.50E-07
8.58E-05 1.36E-05
1.19E-04 1.10E-05
9.78E-05 7.00E·06
2.08E-04 1.00E-05
6.05E-04 1.64E-04
l.lOE-04 8.00E-06
6.10E-05 6.00E-06
1.07E-04 6.00E-06
8.86E-04 1.80E-05
6.66E-04 1.80E-05
5.20E-04 1.00E-04
4.10E-04 l.OOE-04
1.60E-04 3.00E-05
3.60E-04 5.00E-05
2.60E-04 5.00E-05
3.10E-05 1.90E-05
6.20E-04 5.00E-05
3.40E-04 3.00E-05
5.10E-04 6.00E-05
3.60E-04 3.00E-05
1.70E-04 2.00E-05
8.80E-05 1.60E-05
3.00E-04 3.00E-05
3.10E-04 3.00E-05
5.00E-04 4.00E-05
2.00E-05 8.00E-06
6.50E-06 6.00E-06
1.20E-04 4.00E-05
1.80E-05 1.70E-05
5.20E-05 1.90E-05
5.10E-05 2.30E-05
1.20E-04 1.00E-05
3.73E-05 1.60E-06
2.40E-04 1.50E-05
8.40E-05 6.10E-06
1.90E-05 1.50E-06
1.20E-04 6.80E-06
8.30E-05 3.30E-06
3.60E-05 2.50E-06
3.30E-05 2.30E-06
5.40E-06 3.50E-07
8.90E-06 7.20E-07
<9.20E-05 9.20E-05
< 6.50E-08 6.50E-08
4.20E-05 1.00E-06
6.20E-05 l.OOE-06
5.45E-05 1.40E-06
1.10E-04 3.00E-06
3.70E-05 1.00E-06
LLD Pb-210 Pb-210 LLD
uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (1.0E-06)
5.00E-08 7.10E-03 3.00E·04 1.00E-06
5.00E·08 8.30E-04 5.00E·05 1.00E-06
7.00E-06 6.40E-04 5.00E·05 4.00E·05
S.OOE-08 2.20E-04 9.00E-05 l.OOE-07
l.OOE-06 8.00E-05 l.OOE-05 l.OOE-05
2.00E-08 3.53E-04 1.90E-05 1.00E-05
5.00E-06 1.58E-04 1.30E-05 l.OOE-05
2.00E-06 2.16E-03 3.40E-04 3.00E-04
3.00E-09 1.60E·03 7.00E·05 3.00E-08
2.00E-07 2.58E-03 l.lOE-04 3.00E-08
3.00E-06 8.63E-04 4.20E-05 3.00E-05
2.00E-06 5.40E-04 S.OOE-05 5.00E-05
2.00E-06 3.80E-04 3.00E-05 2.00E-05
2.00E-06 4.40E-03 1.90E-04 3.00E-05
3.00E-06 4.78E-03 2.10E-04 6.00E-05
3.00E-06 1.70E-03 l.OOE-04 6.00E-05
5.00E-08 1.60E-03 1.00E-04 1.00E-06
5.00E-08 S.SOE-04 4.00E-05 1.00E-06
5.00E-08 1.80E-03 l.OOE-04 l.OOE-06
5.00E-08 1.90E-03 l.OOE-04 l.OOE-06
5.00E-08 1.60E-04 4.00E-05 l.OOE-06
*** 1.70E-03 l.OOE-04 ***
*** 7.40E-04 3.00E-05 ***
7.00E-06 l.OOE-03 7.00E-05 1.40E-05
4.00E-06 4.80E-04 2.00E-05 2.20E-05
5.00E-08 3.20E-04 2.00E-05 l.OOE-06
S.OOE-08 2.90E-04 2.00E-05 1.00E-06
S.OOE-06 4.10E-04 2.00E-05 l.OOE-06
2.00E-07 4.70E-04 2.00E-05 2.00E-07
5.00E-08 1.50E-03 l.OOE-04 1.00E-06
2.00E-06 9.60E-05 1.40E-05 l.OOE-05
2.00E-06 1.20E-04 2.00E-05 l.OOE-06
3.00E-06 1.21E-03 8.00E-05 2.00E-05
3.00E-06 2.10E-04 3.00E-05 2.00E-05
3.00E-06 1.70E-05 3.60E-05 2.00E-05
3.00E-06 7.10E-04 6.00E-05 2.00E-05
3.00E-05 9.80E-04 1.60E-04 2.00E-04
8.40E-08 7.80E-05 7.10E-06 4.20E-07
1.70E-07 2.60E-04 1.30E-05 8.30E-07
1.50E-07 1.20E-04 l.lOE-05 7.50E-05
1.40E-07 4.50E-05 4.30E-06 7.20E-07
1.40E-07 l.OOE-05 5.80E-06 7.10E-07
1.90E-07 6.80E-05 6.30E-06 1.80E-07
1.60E-07 8.50E-05 5.60E-06 8.40E-07
1.70E-07 4.40E-05 4.80E-06 8.40E-07
1.56E-07 3.20E-05 9.00E-07 7.83E-07
5.40E-07 3.40E-04 6.70E-06 l.lOE-07
9.20E-05 <4.60E-04 4.60E-04 4.60E-04
6.50E-08 <3.20E-07 3.20E-07 3.20E-07
1.10E-07 1.70E-04 1.00E-05 5.50E-07
l.OOE-07 1.40E-04 7.00E-06 l.OOE-07
8.30E-08 9.20E-05 4.00E-06 4.20E-07
2.20E-07 2.80E-05 1.00E-06 l.lOE-06
2.40E-07 2.70E-04 l.OOE-05 1.20E-06
2nd '00 22-Jun-00 2.90E-05 l.OOE-06 3.30E-07 2.80E-04 2.00E-05 1.70E-06
4th '00 21-Dec-00 2.30E-06 1.40E-06 3.70E-07 3.30E-04 S.OOE-05 1.90E-06
1st '01 30-Apr-01 2.10E-05 l.OOE-06 l.SOE-07 <7.6E-07 N/A 7.60E-07
2nd'01 14-Jun-01 1.30E-06 4.00E-08 1.20E-07 1.80E-06 3.00E-08 5.90E-07
4th '01 17-Dec-01 3.70E-05 7.67E-07 8.30E-08 6.72E-05 2.62E-06 6.00E-07
1st '02 07-May-02 4.90E-OS 2.40E-06 7.60E-07 1.28E-04 S.61E-06 l.OOE-OS
2nd'02 07-Jul-02 8.88E-OS 4.32E-06 7.60E-07 8.33E-OS 4.32E-06 l.OOE-OS
4th '02 lS-Dec-02 l.SOE-04 6.20E-06 7.60E-07 3.16E-04 1.07E-OS l.OOE-OS
1st '03 21-Mar-03 S.OOE-OS 3.40E-06 2.71E-06 <4.2e-6 4.20E-06
2nd'03 10-Jun-03 S.60E-OS 2.00E-06 4.10E-07 1.88E-04 5.14E-06 8.20E-08
4th '03 20-Nov-03 3.20E-04 8.20E-06 1.70E-07 4.89E-04 1.2SE-OS 8.30E-07
1st '04 08-Apr-04 6.29E-05 4.10E-06 2.00E-07 1.94E-OS 4.00E-06 l.OOE-06
2nd'04 12-Jun-04 6.S1E-OS 3.40E-06 1.30E-07 1.87E-OS 3.90E-06 6.SOE-07
4th '04 30-Nov-04 7.SOE-OS 4.60E-06 2.00E-08 4.4SE-04 1.40E-OS 3.00E-07
1st 'OS 21-Apr-OS 4.90E-OS 2.70E-06 1.30E-07 1.27E-04 4.80E-06 6.SOE-07
2nd 'OS 13-Jun-OS 2.30E-OS 2.10E-06 l.SOE-07 4.70E-OS 5.10E-06 7.60E-07
4th 'OS 10-Nov-OS 7.40E-OS 3.SOE-06 1.20E-10 2.40E-06 8.10E-08 S.80E-10
1st '06 03-Apr-06 l.OOE-04 6.00E-06 S.OOE-08 6.S4E-04 1.SOE-OS l.OOE-06
2nd '06 16-Jun-06 9.SOE-05 S.90E-06 S.OOE-08 4.48E-04 1.40E-OS l.OOE-06
4th '06 28-Nov-06 8.13E-OS 4.10E-06 2.20E-07 3.2SE-04 1.12E-06 l.OOE-OS
1st '07 30-Mar-07 4.30E-OS 2.60E-06 1.70E-07 2.64E-04 7.20E-06 8.60E-07
2nd '07 1-Jun-07 S.10E-OS 3.20E-06 2.30E-07 S.30E-04 1.40E-06 1.20E-06
4th '07 23-Nov-07 7.30E-OS 6.60E-06 S.OOE-08 7.00E-04 2.20E-OS 1.10E-06
1st '08 22-Apr-08 2.80E-06 2.80E-06 7.20E-07 4.40E-04 2.00E-OS l.OOE-06
2nd'08 18-Jun-08 3.20E-06 3.30E-06 1.80E-06 1.40E-04 3.30E-OS S.SOE-OS
4th '08 12-Dec-08 7.30E-OS 3.20E-06 7.40E-07 4.40E-04 2.SOE-OS 3.20E-OS
1st '09 28-Apr-09 S.2SE-OS 3.60E-06 l.lOE-06 1.90E-04 l.SOE-OS 2.20E-OS
2nd'09 17-Jun-09 2.30E-OS 1.60E-OS S.20E-07 4.30E-OS l.OOE-OS 1.70E-OS
4th '09 18-Dec-09 S.SOE-OS 3.SOE-06 3.00E-04 l.lOE-OS
1st '10 13-May-10 1.90E-04 6.10E-06 9.40E-07 5.10E-04 2.40E-OS 3.10E-OS
2nd'10 18-Jun-10 2.30E-OS 2.00E-06 7.70E-07 8.30E-OS 1.80E-OS 2.90E-OS
4TH '10 20-Dec-10 8.60E-06 9.10E-07 3.90E-07 1.10E-07 6.80E-07 l.lOE-06
2nd'11 23-Jun-11 2.10E-07 1.20E-07 1.40E-07 <2.2E-06 1.30E-06 2.20E-06
2nd'12 11-Apr-12 l.SOE-OS 9.50E-07 2.60E-07 <7.0E-07 6.00E-07 l.OOE-06
.3rd '12 11-Jun-12 8.30E-06 S.40E-07 1.20E-07 1.40E-04 8.30E-06 6.SOE-06
4th '12 06-Nov-12 2.34E-OS 4.10E-07 7.71E-08 4.59E-04 3.83E-06 6.18E-07
2nd'13 30-Apr-13 9.04E-OS 1.68E-06 8.58E-07 2.24E-04 4.46E-06 4.68E-06
3rd '13 20-Jun-13 2.S8E-06 9.59E-07 8.06E-07 1.06E-04 2.30E-06 3.28E-06
*2nd quarter of 1996 San Juan County, Utah, was declared a d1saster area due to drought, no samples were collected dunng th1s penod
WHITE MESA MILL
FORAGE RADIONUCLIDE DATA
SOUTHWEST OF MILL
SAMPLED QTR. SAMPLED DATE
3rd '81 27-Aug-81
4th '81 20-0ct-81
2nd '82 15-Apr-82
3rd '82 01-Jul-82
4th '82 30-Nov-82
2nd '83 13-Apr-83
3rd '83 01-Jui-83
4th '83 30-Jan-84
2nd'84 28-Jun-84
4th '84 14-Nov-84
2nd'85 27-Mar-85
3rd'85 15-Jul-85
4th '85 09-0ct-85
2nd'86 24-Mar-86
3rd '86 10-Jul-86
4th '86 18-Dec-86
2nd '87 20-Apr-87
3rd '87 05-Jun-87
4th '87 22-Dec-87
2nd'88 19-Apr-88
3rd '88 28-Jul-88
2nd'89 07-Apr-89
3rd'89 06-Jun-89
4th '89 07-Nov-89
1st '90 17-Apr-90
2nd '90 20-Jun-90
3rd '90 17-0ct-90
1st '91 10-Apr-91
2nd '91 11-Jun-91
3rd '91 20-Nov-91
1st '92 22-Apr-92
2nd '92 10-Jun-92
3rd'92 10-Jun-92
1st '93 13-Apr-93
2nd'93 26-Jun-93
3rd'93 12-0ct-93
1st '94 11-May-94
2nd'94 19-Jui-94
3rd'94 28-Nov-94
1st '95 11-Apr-95
2nd'95 06-Jul-95
3rd '95 15-Nov-95
1st '96 23-Apr-96
2nd '96 * 31-Jul-96
3rd '96 14-Nov-96
1st '97 21-Apr-97
3rd'97 05-Sep-97
4th '97 20-Nov-97
1st '98 23-Mar-98
2nd'98 16-Jun-98
4th'98 05-Nov-98
2nd '99 15-Apr-99
3rd '99 07-Jul-99
4th'99 02-Dec-99
2nd '00 21-Apr-00
Ra-226 Ra-226
VALUE (uCi/Kg) ERROR (uCi/Kg)
9.50E-04 2.00E-05
3.00E-05 3.00E-06
1.37E-05 3.00E-06
3.40E-04 2.00E-05
1.75E-05 3.00E-06
7.13E-04 7.30E-05
5.39E-05 4.50E-06
6.40E-05 ?.OOE-06
8.27E-05 6.30E-06
2.72E-04 1.48E-04
4.73E-04 1.60E-07
6.60E-05 7.00E-06
2.83E-04 2.00E-05
1.57E-04 l.OOE-05
3.78E-04 l.OOE-05
2.60E-04 2.00E-05
4.10E-04 7.00E-05
2.90E-04 4.00E-05
1.80E-04 3.00E-05
2.30E-04 5.00E-05
1.50E-04 3.00E-05
3.10E-04 4.00E-05
1.30E-04 2.00E-05
4.30E-04 S.OOE-05
2.SOE-04 3.00E-05
l.lOE-04 2.00E-05
6.10E-05 1.40E-05
3.40E-05 l.lOE-05
8.00E-05 6.00E-06
6.50E-05 1.40E-05
l.GOE-05 7.00E-06
1.90E-05 l.OOE-05
l.GOE-05 1.80E-OS
2.60E-05 2.00E-05
3.00E-05 1.40E-05
3.10E-05 l.GOE-05
2.00E-05 5.00E-06
1.75E-05 1.70E-06
l.OOE-04 9.00E-06
1.70E-05 1.50E-06
6.40E-06 6.00E-07
2.30E-05 2.20E-06
4.20E-05 2.20E-06
2.10E-05 2.00E-06
5.50E-06 4.20E-07
5.30E-06 3.20E-07
2.50E-05 9.50E-07
<7.90E-05 7.90E-05
3.60E-07 1.40E-07
4.30E-05 l.OOE-06
2.40E-05 l.OOE-06
2.23E-05 8.60E-07
1.50E-04 3.00E-06
1.00E-04 2.00E-06
LLD Pb-210 Pb-210 LLD
uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCI/Kg) uCi/Kg (l.OE-06)
5.00E-08 l.SOE-04 l.OOE-05 l.OOE-06
5.00E-08 1.50E-04 2.00E-05 l.OOE-06
3.00E-06 3.80E-04 4.00E-05 4.00E-05
5.00E-08 3.68E-03 2.70E-04 l.OOE-07
2.00E-06 7.92E-04 4.00E-06 2.00E-05
9.00E-08 2.51E-03 3.00E-04 3.00E-04
2.00E-06 6.88E-04 4.30E-05 4.00E-05
4.00E-06 1.20E-03 l.OOE-04 4.00E-05
3.00E-09 1.80E-03 l.OOE-04 9.00E-08
2.00E-07 4.70E-03 7.20E-04 3.00E-07
3.00E-06 7.07E-04 3.60E-05 3.00E-05
4.00E-06 4.90E-04 3.00E-05 3.00E-05
7.00E-06 1.50E-03 l.OOE-04 7.00E-05
4.00E-06 4.14E-03 1.80E-04 3.00E-05
2.00E-06 1.65E-02 7.00E-04 l.OOE-04
2.00E-06 1.70E-03 l.OOE-04 1.00E-04
5.00E-08 2.20E-03 l.OOE-04 l.OOE-06
S.OOE-08 7.50E-04 S.OOE-05 l.OOE-06
S.OOE-08 2.40E-03 l.OOE-04 l.OOE-06
5.00E-08 2.90E-03 l .OOE-04 1.00E-06
5.00E-08 4.30E-03 2.00E-04 l.OOE-06
*** 4.20E-03 l.OOE-04 ***
*** 1.50E-03 l.OOE-04 ***
1.40E-05 3.50E-03 1.40E-04 2.70E-05
5.00E-06 2.39E-03 5.00E-05 2.50E-05
5.00E-08 6.60E-04 3.00E-05 l.OOE-06
5.00E-08 6.10E-04 3.00E-05 1.00E-06
5.00E-06 2.20E-04 l.OOE-05 1.00E-06
2.00E-07 1.20E-04 l.OOE-05 2.00E-07
5.00E-08 9.10E-04 5.00E-05 1.00E-06
2.00E-06 3.20E-04 2.00E-05 l.OOE-05
2.00E-07 2.20E-04 2.00E-05 l.OOE-06
3.00E-06 7.60E-04 6.00E-05 2.00E-05
3.00E-06 3.40E-04 3.00E-05 2.00E-05
3.00E-06 O.OOE+OO 3.00E-05 2.00E-05
3.00E-06 4.20E-04 6.00E-05 2.00E-05
3.00E-05 3.90E-04 8.00E-05 2.00E-04
7.60E-08 1.30E-04 7.80E-06 3.80E-07
1.50E-07 2.60E-04 1.20E-05 7.40E-07
l.GOE-07 1.60E-04 1.50E-05 8.10E-07
1.40E-07 4.40E-05 4.20E-06 7.00E-07
1.70E-07 6.60E-05 9.60E-06 8.30E-07
1.70E-07 l.OOE-04 6.70E-06 1.80E-07
l.GOE-07 1.90E-04 7.30E-06 8.20E-07
1.40E-07 3.30E-05 3.90E-06 7.00E-07
1.26E-07 1.90E-05 6.90E-07 6.34E-07
5.90E-07 1.30E-04 4.70E-06 1.20E-07
7.90E-05 <3.90E-04 3.90E-04 3.90E-04
3.30E-08 <1.7E-07 1.70E-07 1.70E-07
7.60E-08 2.50E-04 l.OOE-05 3.80£-07
1.20E-07 1.70E-04 8.00E-06 6.20E-07
1.20E-07 2.30E-04 ?.OOE-06 5.90E-07
2.00E-07 1.70E-05 l .OOE-06 l .OOE-06
1.20E-07 l.lOE-04 ?.OOE-06 6.10E-07
2nd 'DO 22-Jun-00 1.30E-06 l.OOE-07 2.40E-07 2.00E-04 LODE-OS 1.20E-06
4th 'DO 21-Dec-00 1.20E-06 9.00E-07 2.40E-07 1.20E-04 3.00E-OS 1.20E-06
1st '01 30-Apr-01 1.80E-06 l.OOE-07 1.70E-07 <8.3E-07 N/A 8.30E-07
2nd'01 14-Jun-01 2.60E-06 2.00E-07 '9.90E-08 1.10E-06 2.00E-08 S.OOE-07
4th '01 17-Dec-01 2.63E-06 4.60E-OS 1.20E-07 9.40E-OS 3.72E-06 6.00E-07
1st '02 07-May-02 3.SOE-OS 2.20E-06 7.60E-07 1.36E-04 S.61E-06 l.OOE-OS
2nd '02 07-Jul-02 4.02E-OS 2.34E-06 7.60E-07 7.04E-OS 4.11E-06 l.OOE-OS
4th '02 1S-Dec-02 8.10E-OS 3.90E-06 7.60E-07 2.87E-04 8.S4E-06 l.OOE-OS
1st '03 21-Mar-03 3.70E-OS 2.60E-06 2.41E-06 2.69E-OS 2.01E-06 3.73E-06
2nd'03 10-Jun-03 1.30E-OS l.OOE-06 S.20E-07 <l.OOE-07 l.OOE-07
4th '03 20-Nov-03 1.60E-04 1.30E-OS 1.20E-07 1.42E-04 6.42E-06 S.90E-07
1st '04 08-Apr-04 1.40E-04 7.70E-06 1.10E-07 6.10E-06 2.70E-06 S.SOE-07
2nd '04 12-Jun-04 6.S1E-OS 3.20E-06 l.SOE-07 S.27E-OS 4.90E-06 7.60E-07
4th '04 30-Nov-04 8.40E-OS S.70E-06 3.00E-08 3.39E-04 1.60E-OS 3.00E-07
1st 'OS 21-Apr-OS 1.70E-OS 1.60E-06 1.30E-07 4.SOE-OS 3.SOE-06 6.SOE-07
2nd'OS 13-Jun-OS 1.SOE-OS 1.60E-06 1.40E-07 7.00E-OS S.10E-06 6.90E-07
4th 'OS 10-Nov-OS 3.80E-OS 2.10E-06 8.60E-10 1.20E-06 4.80E-08 4.30E-10
1st '06 03-Apr-06 1.00E-04 6.00E-06 S.OOE-08 3.30E-04 l.lOE-OS l.OOE-06
2nd '06 16-Jun-06 3.40E-OS 2.SOE-06 S.OOE-08 1.37E-04 6.00E-06 l.OOE-06
4th '06 28-Nov-06 7.31E-OS 3.20E-06 1.60E-07 2.98E-04 8.SOE-06 8.20E-07
1st '07 30-Mar-07 3.00E-OS 2.20E-06 1.70E-07 3.20E-04 7.90E-06 8.40E-07
2nd'07 1-Jun-07 1.10E-04 4.60E-06 2.3-07 3.20E-04 1.10E-OS l.lOE-06
4th '07 23-Nov-07 S.60E-OS S.20E-06 S.OOE-08 6.40E-04 1.90E-OS 1.00E-06
1st '08 22-Apr-08 3.20E-OS 2.30E-06 7.20E-07 2.30E-04 l.SOE-OS l.OOE-06
2nd '08 18-Jun-08 1.2SE-OS 2.20E-06 1.80E-06 S.OOE-OS 3.00E-OS 4.80E-03
4th '08 12-Dec-08
1st '09 28-Apr-09 2.60E-OS 2.90E-06 1.40E-06 3.70E-OS l.SOE-06 2.50E-OS
2nd'09 17-Jun-09 2.40E-OS 1.40E-06 3.90E-07 3.SOE-OS 7.90E-06 1.30E-OS
4th '09 18-Dec-09 3.10E-OS 2.30E-06 2.10E-04 8.40E-06
1st '10 13-May-10 2.00E-OS 2.10E-06 9.40E-07 S.60E-OS 1.SOE-05 2.40E-05
2nd '10 18-Jun-10 l.lOE-05 1.30E-06 6.60E-07 7.80E-05 1.60E-05 2.50E-05
4th '10 20-Dec-10 6.70E-06 9.10E-07 4.80E-07 8.00E-07 7.90E-07 1.30E-06
2nd'll 23-Jun-11 <1.7E-07 6.90E-08 1.70E-07 <2.5E-06 1.50E-06 2.50E-06
2nd '12 11-Apr-12 5.00E-06 6.00E-07 3.00E-07 <7.0E-07 7.00E-07 l.OOE-06
3rd '12 11-Jun-12 1.90E-08 6.20E-08 l.lOE-07 <2.5E-07 1.30E-06 2.20E-06
4th '12 06-Nov-12 1.49E-05 3.41E-07 4.25E-08 4.45E-04 4.01E-06 8.57E-07
2nd '13 30-Apr-13 4.50E-05 1.19E-06 5.39E-07 3.62E-04 6.30E-06 9.90E-06
3rd '13 20-Jun-13 1.51E-05 1.06E-06 1.96E-06 6.71E-05 2.93E-06 6.24E-06
*2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period
C$141 1 Laboratories LLc
a member of The GEL Group INC PO Box 30712 Charleston, SC 29417
2040 Savage Road Charleston, SC 29407
P 843.556.8171 F 843.766.1178
May 28,2013
Ms. Kathy Weinel
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Re: Vegetation Analysis
Work Order: 325082
Dear Ms. Weinel:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on May 03, 2013. This original data report has been prepared and reviewed in accordance
with GEL's standard operating procedures.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 4505.
Purchase Order: DW16138
Enclosures
Sincerely
Heather Shaffer
Project Manager
111111111111111111111111
www.gel.com
Energy Fuels Resources (USA), Inc.
Vegetation Analysis
SDG: 325082
Case Narrative
Page 1 of 19
Page 2 of 19
May 28,2013
Laboratory Identification:
GEL Laboratories LLC
2040 Savage Road
Charleston, South Carolina 29407
[phone]
Summary:
Receipt Narrative
for
Energy Fuels Resources (USA), Inc.
SDG: 325082
Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on May 03, 2013
for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample
containers arrived without any visible signs of tampering or breakage. The lab requested additional volume for
the North West location ..
Sample Identification: The laboratory received the following samples:
Laboratory ID Client ID
325082001 North East
325082002 North West
325082003 South West
Case Narrative:
Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any
technical or administrative problems during analysis, data review, and reduction are contained in the analytical
case narratives in the enclosed data package.
The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler
Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry.
Heather Shaffer
Project Manager
Page 3 of 19
Chain of Custody and
Supporting
Documentation
Sheet 1 of 1
....
CHAIN OF CUSTODY
Samples Shipped to: Gel Laboratories Contact: Garrin Palmer
~~~~~~---------2040 Savage Rd Ph: 435 678 2221
Charleston, South Carolina 29407 [e-mail]
Chain of Custody/Sampling Analysis Request
p . roject Sa mp1ers N a me s _amplers_ 51 1gnature
Early Spring Vegetation c~ t?~ 2013 Garrin Palmer
Date Time
SampleiD Collected Collected
North East 4/30/2013 1200 RA 226, PB-210
North West 4/30/2013 1245 RA 226, PB-211
South West 4/30/2013 1400 RA 226, PB-212
Comments:
Aelihqulshed By:'(Signature)· Oat elf;: Ref:d By:(Signature) Datefrime ~-~ .'1/~11·$
r A/JYtf-5-3--13 ' e:'0A---tf"", ~ /OCv 69t20
Relinquished By:(Signature) Date/Tfme Received By:(Signature) Datefrime
Page 4 of 19
mD I Laboratories u_c
2
2a Daily check performed and passed on
IR temperature gun?
3 Chain of custody documents included
with shipment?
4 Sample containers intact and sealed?
s
6 VOA vials free of headspace (defined
< 6mm bubble}?
7
8 received within holding
9 !D's on COC match !D's on
Date & time on COC match date & 10 time on bottles?
Number of containers received match 11 number indicated on COC?
12 Are sample containers identifiable as
provided?
13 fonn is properly signed in
inquished/received sections?
14 Carrier and tracking number.
Page 5 of 19
SAMPLE RECEIPT & REVIEW FORM
Items)
Seals broken Damaged container Leaking container
Preservation Method: Ice bags Blue ice Dry Ice~ Other (describe)
•alltempemtures are recorded in Celsius
TemperJture Device Serial# (If Applicable): (p { s ~ l{-~L~
Applicublc~
Seals broken Damaged container Leaking container Other (describe)
!D's, containers affected and observed pH:
Circle 1\JJJJm;uo''"
FedEx Air FedEx Ground UPS Field Services Courier Other
\Z.
GEL Laboratories LLC -Login Review Report Report Date: 28-MAY-13
Work Order: 325082
Page 1 of 2
GEL Work Order/SDG: 325082
Client SDG: 325082
Early Spring Vegetation 2013 Work Order Due Date: 02-JUN-13 Collector: C
Project Manager:
Project Name:
Purchase Order:
Package Level:
EDD Format:
Heather Shaffer
DNMI00101 Vegetation Analysis
DW16138
LEVEL3
EIM_DNMI
GELID Client Sample ID Client Sample Desc.
325082001 North East
325082002 North West
325082003 South West
Client Sample ID
-001 North East
-002 North West
-003 South West
Status Tests/Methods
REVW GFPC, Total Alpha Radium, solid
REVW GFPC, Pb210, Solid
REVW GFPC, Total Alpha Radium, solid
REVW GFPC, Pb21 0, Solid
REVW GFPC, Total Alpha Radium, solid
REVW GFPC, Pb210, Solid
Collect
Date & Time
30-APR-13 12:00
30-APR-13 12:45
30-APR-13 14:00
Product
Reference
Package Due Date:
EDD Due Date:
Due Date:
HXS1
Receive Time #of
Date & Time Zone Cont.
03-MAY-13 09:20 -2 1
03-MAY-13 09:20 -2 1
03-MAY-13 09:20 -2 1
Fax Date PM Comments
Product: GFC_PBS Workdef ID: 1310600 In Product Group? No Group Name:
Method: DOE RP280 Modified
Product Description: GFPC, Pb210, Solid
Samples: 001 , 002, 003
Parmname Check: All parmnames scheduled properly
CAS# Parmname
14255-04-0 Lead-210
Client RDL or
PQL & Unit
.000001
30-MAY-13
01-JUN-13
02-JUN-13
Prelogin #: 20130503139
Project Workdef ID: 1310529
SDG Status: Closed
Logged by:
Lab Fax Days to Prelog Lab Field
Matrix Due Date Process CofC#
VEGETATION 30
VEGETATION 30
VEGETATION 30
Aux Data
Client Matrix
Cooler Seal Undisturbed
Temperature (C)
Client Matrix
Cooler Seal Undisturbed
Temperature (C)
Client Matrix
Cooler Seal Undisturbed
Temperature (C)
Group Reference:
SOLID
y
17
SOLID
y
17
SOLID
y
17
Path: Standard
Product Reference:
Group QC QC
1
Receive
Codes
Moisture Correction: "As Received"
Reporting
Units
uCi/kg
Parm Included Included Custom
Function in Sample? in QC? List?
REG y y Yes
0\ -4-; 0
\0
Q) on <:e A..
GEL Laboratories LLC -Login Review Report
Product: GFCTORAS Workdef ID: 1310679
Method: EPA 900.1 Modified
Product Description: GFPC, Total Alpha Radium, solid
Samples: 001, 002, 003
Parmname Check: All parmnames scheduled properly
CAS# Parmname
Total Radium
In Product Group? No
Action Product Name Description
Contingent
Tests
Login Requirements:
Requirement
Group Name:
Client RDL or
PQL & Unit
.00000005
Samples
Group Reference:
Report Date: 28-MAY-13
Work Order: 325082
Page 2 of 2
Path: Standard
Product Reference:
Moisture Correction: "As Received"
Reporting Parm Included Included Custom
Units Function in Sample? in QC? List?
uCifkg REG y y Yes
Include? Comments
Peer Review by: ____________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location?-----~
0\ -.......
0
r--
Q)
~ 0-.
Page 8 of 19
Laboratory
Certifications
List of current GEL Certifications as of 28 May 2013
State Certification
Alaska UST-110
Arkansas 88-0651
CLIA 4200904046
California NELAP 01151CA
Colorado SC00012
Connecticut PH-0169
Delaware SC00012
DoD ELAP A2LA ISO 17025 2567.01 --Florida NELAP E87156
Foreign Soils Permit P330-12-00283,P330-12-00284
Georgia SC00012
Georgia SOW A 967
Hawaii SC00012
Idaho SC00012
Illinois NELAP 200029
Indiana C-SC-01
Kansas NELAP E-10332
Kentucky 90129
Louisiana NELAP 03046 (AI33904)
Louisiana SDWA LA130005
Maryland 270
Massachusetts M-SC012
Nevada SC000122011-I
New Hampshire NELAP 2054
New Jersey NELAP SC002 ..
New Mexico SC00012
New York NELAP 11501
North Carolina 233
North Carolina SDWA 45709
Oklahoma 9904
Pennsylvania NELAP 68-00485
Plant Material Permit PDEP-12-00260
South Carolina Chemistry 10120001
South Carolina Radiochemi 10120002
Tennessee TN 02934
Texas NELAP T1 04 704235-13-8
UtahNELAP SC000122013-8
Vermont VT87156
Virginia NELAP 460202
Washington C780-12
Wisconsin 999887790
Page 9 of 19
Page 10 of 19
Radiochemistry Case Narrative
Energy Fuels Resources (DNMI)
SDG 325082
Method/Analysis Information
Product: GFPC, Total Alpha Radium, solid
Analytical Method: EPA 900.1 Modified
Prep Method: Dry Soil Prep
Analytical Batch Number: 1299872
1299423 Prep Batch Number:
Sample ID Client ID
325082001 North East
325082002 North West
325082003 South West
1202871051 Method Blank (MB)
1202871052 325082003(South West) Sample Duplicate (DUP)
1202871053 325082003(South West) Matrix Spike (MS)
1202871054 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
SOP Reference
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with
GL-RAD-A-010 REV# 15.
Calibration Information:
Calibration Information
All initial and continuing calibration requirements have been met.
Standards Information
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
before the expiration dates.
Sample Geometry
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control (OC) Information:
Blank Information
The blank volume is representative of the sample volume in this batch.
Page 11 of 19
Designated QC
The following sample was used for QC: 325082003 (South West).
QC Information
All of the QC samples meet the required acceptance limits with the following exceptions: The blank,
1202871051 (MB), did not meet the detection limit due to keeping the blank volume consistent with the other
sample aliquots. All other samples met the detection limits. The sample and the duplicate, 1202871052 (South
West) and 325082003 (South West), did not meet the relative percent difference requirement; however, they do
meet the relative error ratio requirement with value of 2.7927. The blank, 1202871051 (MB ), result is greater
than the required detection limit but less than the MDC.
Technical Information:
Holding Time
All sample procedures for this sample set were performed within the required holding time.
Sample Re-prep/Re-analysis
Samples were recounted due to low recovery. The recounts are reported.
Chemical Recoveries
All chemical recoveries meet the required acceptance limits for this sample set.
Miscellaneous Information:
Data Exception (DER) Documentation
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
SOP or contractual documents. A data exception report (DER) was not generated for this SDG.
Additional Comments
The matrix spike, 1202871053 (South West), aliquot was reduced to conserve sample volume.
Qualifier Information
Manual qualifiers were not required.
Method/Analysis Information
Product: GFPC, Pb210, Solid
Analytical Method: DOE RP280 Modified
Prep Method: Dry Soil Prep
Analytical Batch Number: 1299873
Prep Batch Number: 1299423
Sample ID
325082001
325082002
325082003
Client ID
North East
North West
South West
Page 12 of 19
1202871055
1202871056
1202871057
1202871058
Method Blank (MB)
325082003(South West) Sample Duplicate (DUP)
325082003(South West) Matrix Spike (MS)
Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
SOP Reference
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with
GL-RAD-A-018 REV# 13.
Calibration Information:
Calibration Information
All initial and continuing calibration requirements have been met.
Standards Information
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
before the expiration dates.
Sample Geometry
All counting sources were prepared in the same geometry as the calibration standards.
Ouality Control (OC) Information:
Blank Information
The blank volume is representative of the sample volume in this batch.
Designated QC
The following sample was used for QC: 325082003 (South West).
QC Information
All of the QC samples meet the required acceptance limits with the following exceptions: The blank 1202871055
(MB) activity is greater than the MDC but is less than five percent of the lowest activity in the batch.
Technical Information:
Holding Time
All sample procedures for this sample set were performed within the required holding time.
Sample Re-prep!Re-analysis
None of the samples in this sample set required reprep or reanalysis.
Chemical Recoveries
All chemical recoveries meet the required acceptance limits for this sample set.
Miscellaneous Information:
Data Exception (DER) Documentation
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
SOP or contractual documents. A data exception report (DER) was not generated for this SDG.
Additional Comments
Additional comments were not required for this sample set.
Page 13 of 19
Qualifier Information
Manual qualifiers were not required.
Certification Statement
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 14 of 19
GEL LA BORA TORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Qualifier Definition Report
for
DNMIOOI Energy Fuels Resources (USA), Inc.
Client SDG: 325082 GEL Work Order: 325082
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a surrogate compound
U Analyte was analyzed for, but not detected above the CRDL.
ReviewN ali dation
GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-Iike deliverables
receive a third level review of the fractional data package.
The following data validator verified the information presented in this data report:
Signature: ~~ Name: Kate Gellatly
Date: 06 JUN 2013 Title: Analyst I
GEL LA BORA TORIES LLC
2040 Savage Road Charleston SC 29407-[phone]-www.gel.com
Certificate of Analysis
Report Date: June 6, 2013
Company:
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
SampleiD:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Vegetation Analysis
North East
325082001
SOLID
30-APR-13 12:00
03-MAY-13
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Pb210, Solid "As Received"
MDC
Lead-210 0,000265 +/-4.41E-06 5 37E-06
GFPC, Total Alpha Radium, solid "As Received"
Total Radium 0.000114 +/-l.74E-06 5 34E-07
The following Prep Methods were erformed:
Method Description
Dry Soil Prep Dry Soil Prep GL-RAD-A,021
The following Analytical Methods were performed:
Method Descrip!i.Q!!.__
DOE RP280 Modified
2 EPA 900 I Modified
Surrogate/Tracer Recovery
Lead Carrier
Barium Carrier
Notes:
Test
GFPC, Pb210, Solid "As Received"
GFPC, Total Alpha Radium, solid "As Received"
RL
l OOE-06
5.00E-08
Analyst
LYTI-
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
Page 15 of 19
Project:
Client ill:
DNMI00101
DNMI001
Units DF Analyst Date Time Batch Method
uCi/kg
uCilkg
Date
05/03/13
Result
KDFl 06/05/13 0805 1299873
KDFl 06/03/13 1021 1299872
Time Prep Batch
1510 1299423
Analyst Comments
Nominal Recovel2'% Acceptable Limits
103
80.9
(25%-125%)
(25%-125%)
2
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: June 6, 2013
Company:
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Vegetation Analysis
North West
325082002
SOLID
30-APR-13 12:45
03-MAY-13
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Pb2l0, Solid "As Received"
MDC
Lead-210 0_000224 +/-4,46£-06 4.68E-06
GFPC, Total Alpha Radium, solid "As Received"
Total Radium 9.04E-05 +/-1.68E-06 8 58E-07
The following Prep Methods were performed:
Method Descripti n
D . Soil Prep Dry Soil Prep GL-RAD-A-021
RL
l .OOE-06
S.OOE-08
nalyst
LYTl-
The following Analytical Methods were performed: ___ ~ ____ _
Metho_d__ Descri tion
2
DOE RP280 Modified
EPA 900.1 Modified
Surrogate/Tracer Recovery Test ---"---Lead Carrier GFPC, Pb210, Solid "As Received"
Barium Carrier GFPC, Total Alpha Radium, solid "As Received"
Notes:
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
Page 16 of 19
Project:
Client ID:
DNMI00101
DNMI001
Units DF Analyst Date Time Batch Method
uCi/kg
uCi/kg
Date
05/03/13
KDFl 06/04/13 1803 1299873
KDFl 06/03/13 1021 1299872
Time
1510
Prep Batch
ff94i3
____ Anal_yst Comments
Result Nominal Recovery%
112
90.0
Acce table Limits
(25%-125%)
(25%-125%)
2
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: June 6, 2013
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
SampleiD:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Vegetation Analysis
South West
325082003
SOLID
30-APR-13 14:00
03-MAY-13
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Pb210, Solid "As Received"
MDC
Lead-21 0 0.000362 +/-6.30E-06 9.90E-06
GFPC, Total Alpha Radium, solid "As Received"
Total Radium 4 50E-05 +/-1 19E-06 5 39E-07
The following Prep Methods were performed:
RL
LOOE-06
5.00E-08
Method D cri t ion
Dry Soil Prep Dry Soil Prep GL-RAD-A-U21
Analyst
--LYTI
The following Analytical Methods were performed: ----Method ___ Description
DOE RP280 Modified
2 EPA 900. I Modified
Test Surrqgate/Tracer Recovery
Lead Carrier GFPC, Pb210, Solid "As Received"
Barium Carrier GFPC, Total Alpha Radium, solid "As Received"
Notes:
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
Page 17 of 19
Project:
Client ID:
DNMI00101
DNMIOOl
Units DF Analyst Date Time Batch Method
uCi/kg
uCi/kg
Date
05/0311_3_
KDF1 06/04/13 1803 1299873
KDFI 06/03/13 1021 1299872
Time Prep Batch
ISI-;;-0 ---,1:-:;:2~99423
Anal st Comments
Result
108
92_6
(25%-125%)
(25%-125%)
2
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407-[phone] -www.gel.com
QC Summary
Contact:
Workorder:
Parmname
Rad Gas Flow
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado
Ms. Kathy Weinel
325082
NOM
Batch 1299872
QCJ202871052 325082003 DUP
Total Radium 4.50E-05
Uncertainty +/-1.19E-06
QC1202871054 LCS
Total Radium 0.00163
Uncertainty
QC1202871051 MB
Total Radium
Uncertainty
QCJ202871053 325082003 MS
Total Radium 0.00226 4.50E-05
Uncertainty +/-1.19E-06
Batch 1299873
QC1202871 056 325082003 DUP
Lead-210 0.000362
Uncertainty +/-6.30E-06
QC1202871058 LCS
Lead-210 0.0662
Uncertainty
QC1202871055 MB
Lead-210
Uncertainty
QC1202871057 325082003 MS
Lead-210 0.0909 0.000362
Uncertainty +/-6.30E-06
Notes:
u
Counting Uncertainty is calculated at the 68% confidence level (I -sigma).
The Qualifiers in this report are defined as follows:
**
<
>
Analyte is a surrogate compound
Result is less than value reported
Result is greater than value reported
The TIC is a suspected aldol-condensation product
QC Units
3.46E-05 uCi/kg
+/-9.66E-07
0.00168 uCi/kg
+/-1 . 78E-05
2.23E-07 uCi/kg
+/-1.98E-07
0.00184 uCi/kg
+/-2.25E-05
0.000324 uCi/kg
+/-5.67E-06
0.0584 uCi/kg
+/-0.000 176
6.16E-06 uCi/kg
+/-1.69E-06
0.0794 uCi/kg
+/-0.000239
RPD%
26.1 *
11.3
A
B
BD
c
D
F
H
For General Chemistry and Organic analysis the target analyte was detected in the associated blank.
Results are either below the MDC or tracer recovery is low
Analyte has been confirmed by GC/MS analysis
Results are reported from a diluted aliquot of the sample
Estimated Value
Analytical holding time was exceeded
Page 18 of 19
Report Date: June 6, 2013
Page 1 of 2
REC% Ran e Anlst
(0%-20%) KDF1
103 (75%-125%)
79.5 (75%-125%)
(0%-20%) KDF1
88.2 (75%-125%)
86.9 (75%-125%)
Date Time
06/03/13 09:42
06/03/13 09:33
06/02/13 18:08
06/02/13 17:21
06/04/13 18:03
06/04/13 08:40
06/04/13 18:03
06/04/13 08:40
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407-[phone] -www.gel.com
QC Summary
Workorder: 325082
Parmname NOM Sample Qual QC Units RPD%
K Analyte present. Reported value may be biased high. Actual value is expected to be lower.
L Analyte present. Reported value may be biased low. Actual value is expected to be higher.
M M if above MDC and less than LLD
M Matrix Related Failure
NIA RPD or %Recovery limits do not apply.
See case narrative
Analyte concentration is not detected above the detection limit
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
Sample results are rejected
Analyte was analyzed for, but not detected above the CRDL.
Gamma Spectroscopy--Uncertain identification
Gamma Spectroscopy--Uncertain identification
REC%
Page 2 of 2
Rang~nlst
Nl
ND
NJ
Q
R
u
UI
UJ
UL
X
y
Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
h
QC Samples were not spiked with this compound
RPD of sample and duplicate evaluated using +/-RL. Concentrations are <SX the RL. Qualifier Not Applicable for Radiochemistry.
Preparation or preservation holding time was exceeded
N/ A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more.
Date Time
1\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/-the
RL is used to evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
Page 19 of 19
mWII I Laboratories LLC
a member of The GEL Group INC PO Box 30712 Charleston, SC 29417
2040 Savage Road Charleston, SC 29407
P 843.556.8171 F 843.766.1178
July 18,2013
Ms. Kathy Weinel
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Re: Vegetation Analysis
Work Order: 328139
Dear Ms. Weinel:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on June 24, 2013. This original data report has been prepared and reviewed in accordance
with GEL's standard operating procedures.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 4505.
Purchase Order: DW16138
Enclosures
Sincerely
Heather Shaffer
Project Manager
www.gel.com
Energy Fuels Resources (USA), Inc.
Vegetation Analysis
SDG: 328139
Case Narrative
Page 1 of 19
Page 2 of 19
July 18, 2013
Laboratory Identification:
GEL Laboratories LLC
2040 Savage Road
Charleston, South Carolina 29407
[phone]
Summary:
Receipt Narrative
for
Energy Fuels Resources (USA), Inc.
SDG: 328139
Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on June 24, 2013
for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample
containers arrived without any visible signs of tampering or breakage. There are no additional comments
concerning sample receipt.
Sample Identification: The laboratory received the following samples:
Laboratory ID Client ID
328139001 North West
328139002 ·North East
328139003 South West
Case Narrative:
Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any
technical or administrative problems during analysis, data review, and reduction are contained in the analytical
case narratives in the enclosed data package.
The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler
Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry.
Heather Shaffer
Project Manager
Page 3 of 19
Chain of Custody and
Supporting
Documentation
Sheet 1 of 1
CHAIN OF CUSTODY
Samples Shipped to: Gel Laboratories Contact: Garrln Palmer
~~~~~~----------2040 Savage Ad Ph: 435 678 2221
Charleston, South Carolina 29407 [e-mail]
Chain of Custody/Sampling Analysis Request
Project
Late Spring Vegetation
Sampling 2013
Date
Sample 10 Collected
North West 6/20/2013
North East 6/2012013
South West 6/20/20.13
"
Comments:
Relinquished By:(Signature) /' n· R u ~ ~ ..... c,tA..A.--
Relinquished By:(Signature)
Page 4 of 19
Sam~ers Name Samplers Signature
Garrin Palmer {r~ ?~tv-
Time
Collected Laboratory Analysis Requested
930 Ra 226, P8-21 0
900 Ra 226, PB-21 0
830 Ra 226, PB-21 0
-
-
m:il Laboratories LLC SAMPLE RECEIPT & REVIEW FORM
Seals broken Damaged container Leaking container Other (describe)
Preservation Method: Ice bags Blue ice Dry
•au temperatures are recorded in
Device Serial N:
ISec:onclarv Temperature Device
Circle
containers intact and sealed? Seals broken Damoged container Leaking container Other (describe)
ID's, conUiinen; affected and observed pH: s
6 VOA vials free of headspacc (defined
as< 6mm bubble)?
ID's on COC match ID's on
FedEx Air FedEx Ground UPS Field Services Courier Other
14 Carrier and tracking number.
Comments (Use
Page 5 of 19
GEL Laboratories LLC -Login Review Report Report Date: 18-JUL-13
Work Order:328139
Page 1 of 2
GEL Work Order/SDG: 328139
Client SDG: 328139
Late spring vegetation 2013 Work Order Due Date: 24-JUL-13 Collector: C
Project Manager:
Project Name:
Purchase Order:
Package Level:
EDD Format:
Heather Shaffer
DNMI001 01 Vegetation Analysis
DW16138
LEVEL3
EIM_DNMI
GELID Client Sample ID Client Sample Desc.
328139001 North West
328139002 North East
328139003 South West
Client Sample ID
-001 North West
-002 North East
-003 South West
Status Tests/Methods
REVW GFPC, Total Alpha Radium, solid
REVW GFPC, Pb210, Solid
REVW GFPC, Total Alpha Radium, solid
REVW GFPC, Pb210, Solid
REVW GFPC, Total Alpha Radium, solid
REVW GFPC, Pb210, Solid
Collect
Date & Time
20-JUN-13 09:30
20-JUN-13 09:00
20-JUN-13 08:30
Product
Reference
Package Due Date:
EDD Due Date:
Due Date:
HXS1
Receive Time #of
Date & Time Zone Cont.
24-JUN-13 10:15 -2 1
24-JUN-13 10:15 -2 I
24-JUN-13 10:15 -2 I
Fax Date PM Comments
Product: GFC_PBS VVorkdefiD: 1310600 In Product Group? No Group Name:
Method: DOE RP280 Modified
Product Description: GFPC, Pb210, Solid
Samples: 001, 002, 003
Parmname Check: All parmnames scheduled properly
CAS# Parmname
14255-04-0 Lead-210
Client RDL or
PQL & Unit
.000001
21-JUL-13
23-JUL-13
24-JUL-13
Prelogin #: 20130604845
Project Workdef ID: 1310529
SDG Status: Closed
Logged by:
Lab Fax Days to Prelog Lab Field
Matrix Due Date Process CofC#
VEGETATION 30
VEGETATION 30
VEGETATION 30
Aux Data
Cooler Seal Undisturbed
Temperature (C)
Cooler Seal Undisturbed
Temperature (C)
Cooler Seal Undisturbed
Temperature (C)
Group Reference:
y
20
y
20
y
20
Path: Standard
Product Reference:
Group QC QC
1
Receive
Codes
Moisture Correction: "As Received"
Reporting
Units
uCi/kg
Parm Included
Function in Sample?
REG y
Included Custom
in QC? List?
y Yes
0\ .-
'-+-< 0
\0
Q) on ~ 0-.
GEL Laboratories LLC -Login Review Report
Product: GFCTORAS Workdef ID: 1310679
Method: EPA 900.1 Modified
Product Description: GFPC, Total Alpha Radium, solid
Samples: 001, 002, 003
Parmname Check: All parmnames scheduled properly
CAS# Parmname
Total Radium
In Product Group? No
Action Product Name Description
Contingent
Tests
Login Requirements:
Requirement
Are these vegetation sample?
Login Reminder?
Group Name:
Client RDL or
PQL & Unit
.00000005
Samples
Group Reference:
Report Date: 18-JUL-13
Work Order: 328139
Page 2 of 2
Path: Standard
Product Reference:
Moisture Correction: "As Received"
Reporting Parm Included Included Custom
Units Function in Sample? in QC? List?
uCi/kg REG y y Yes
Include? Comments
y
y
FOR VEGETATION: After logging in, change from DRY to WET in sample inquiry.
FOR VEGETATION: After logging in, change from DRY to WET in sample inquiry.
Peer Review by: ___________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? _____ _
0\ ........
........
0
r--
Cl)
bll ell 0...
Page 8 of 19
Laboratory
Certifications
List of current GEL Certifications as of 18 July 2013
State Certification
Alaska UST-110
Arkansas 88-0651
CLIA 42D0904046
California NELAP OIL SICA
Colorado SCOOOI2
Connecticut PH-0169
Delaware SCOOOI2
DoD ELAP A2LA ISO 17025 2567.01
Florida NELAP E87156
Foreign Soils Permit P330-12-00283,P330-12-00284
Georgia SC00012
Georgia SDWA 967
Hawaii SC00012
Idaho SCOOOI2
Illinois NELAP 200029
Indiana C-SC-01
Kansas NELAP E-10332
Kentucky 90129
Louisiana NELAP 03046 (AI33904)
Louisiana SDWA LAI30005
Maryland 270
Massachusetts M-SCOI2
Nevada SC000122011-I
New Hampshire NELAP 2054
New Jersey NELAP SC002 --New Mexico SC00012
New York NELAP 11501
North Carolina 233
North Carolina SDWA 45709
Oklahoma 9904
Pennsylvania NELAP 68-00485
Plant Material Permit PDEP-12-00260
South Carolina Chemistry 10120001
South Carolina Radiochemi 10120002
Tennessee TN 02934
TexasNELAP T104704235-13-8
UtahNELAP SC000122013-8
Vermont VT87156
Virginia NELAP 460202
Washington C780-12
Wisconsin 999887790
Page 9 of 19
Page 10 of 19
Method/ Analysis Information
Radiochemistry Case Narrative
Energy Fuels Resources (DNMI)
SDG 328139
Product: GFPC, Total Alpha Radium, solid
Analytical Method: EPA 900.1 Modified
Prep Method: Dry Soil Prep
Analytical Batch Number: 1310694
Prep Batch Number: 1310207
Sample ID
328139001
328139002
328139003
1202899156
1202899157
1202899158
1202899159
Client ID
North West
North East
South West
Method Blank (MB)
328139002(North East) Sample Duplicate (DUP)
328139002(North East) Matrix Spike (MS)
Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
SOP Reference
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with
GL-RAD-A-010 REV# 15.
Calibration Information:
Calibration Information
All initial and continuing calibration requirements have been met.
Standards Information
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
before the expiration dates.
Sample Geometry
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control (OC) Information:
Blank Information
The blank volume is representative of the sample volume in this batch.
Page 11 of 19
Designated QC
The following sample was used for QC: 328139002 (North East).
QC Information
All of the QC samples meet the required acceptance limits with the following exceptions: The blank,
1202899156 (MB), did not meet the detection limit due to keeping the blank volume consistent with the other
sample aliquots. All other samples met the detection limits. The blank 1202899156 (MB) result is greater than
the required detection limit but less than the MDC.
Technical Information:
Holding Time
All sample procedures for this sample set were performed within the required holding time.
Sample Re-prep/Re-analysis
None of the samples in this sample set required reprep or reanalysis.
Chemical Recoveries
All chemical recoveries meet the required acceptance limits for this sample set.
Miscellaneous Information:
Data Exception (DER) Documentation
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
SOP or contractual documents. A data exception report (DER) was not generated for this SDG.
Additional Comments
Additional comments were not required for this sample set.
Qualifier Information
Manual qualifiers were not required.
Method/ Analysis Information
Product: GFPC, Pb210, Solid
Analytical Method: DOE RP280 Modified
Prep Method: Dry Soil Prep
Analytical Batch Number: 1310699
Prep Batch Number: 1310207
Sample ID Client ID
328139001 North West
328139002 North East
328139003 South West
1202899166 Method Blank (MB)
1202899167 328139002(North East) Sample Duplicate (DUP)
Page 12 of 19
1202899168 328139002(North East) Matrix Spike (MS)
1202899169 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
SOP Reference
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with
GL-RAD-A-018 REV# 13 .
Calibration Information;
Calibration Information
All initial and continuing calibration requirements have been met.
Standards Information
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
before the expiration dates.
Sample Geometry
All counting sources were prepared in the same geometry as the calibration standards.
Ouality Control (OC) Information:
Blank Information
The blank volume is representative of the sample volume in this batch.
Designated QC
The following sample was used for QC: 328139002 (North East).
QC Information
All of the QC samples meet the required acceptance limits with the following exceptions: The blank,
1202899166 (MB), did not meet the detection limit due to keeping the blank volume consistent with the other
sample aliquots. All other samples met the detection limits.
Technical Information:
Holding Time
All sample procedures for this sample set were performed within the required holding time.
Sample Re-prep!Re-analysis
Samples were recounted due to a suspected blank false positive. The recounts are reported.
Chemical Recoveries
All chemical recoveries meet the required acceptance limits for this sample set.
Miscellaneous Information:
Data Exception (DER) Documentation
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
SOP or contractual documents. A data exception report (DER) was not generated for this SDG.
Additional Comments
Additional comments were not required for this sample set.
Page 13 of 19
Qualifier Information
Manual qualifiers were not required.
Certification Statement
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 14 of 19
GEL LA BORA TORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Qualifier Definition Report
for
DNMI001 Energy Fuels Resources (USA), Inc.
Client SDG: 328139 GEL Work Order: 328139
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a surrogate compound
U Analyte was analyzed for, but not detected above the CRDL.
ReviewN alidation
GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables
receive a third level review of the fractional data package.
The following data validator verified the information presented in this data report:
Signature: 9l 0 0...J.)...u ~ · 1'-t <... ( C...@ (I rJ
Date: 02 AUG 2013
Name: Heather McCarty
Title: Analyst II
GEL LA BORA TORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: August 2, 2013
Parameter
Company :
Address:
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Vegetation Analysis
North West
328139001
Vegetation
20-JUN-13 09:30
24-JUN-13
Client
Qualifier Result Uncertainty MDC RL
Project:
Client ID:
DNMI00101
DNMI001
Units DF Analyst Date Time Batch Method ------------------Rad Gas Flow Proportional Counting
GFPC, Pb210, Solid "As Received"
Lead-21 0 0 000 I 06 +/-2.30E-06 3 28E-06
GFPC, Total Alpha Radium, solid "As Received"
Total Radium 2.58E-05 +/-9.59E-07 8 06E-07
The following Prep Methods were performed:
I OOE-06
5.00E-08
Method Description
=-:=-c-==-c---=--=-o Dry Soil Prep Dry Soil Prep GL-RAD-A-021
Analyst ------ex=· 'CI
The following Analytical Methods were performed:
Method Description
I DOE RP280 Modified
2 EPA 900 I Modified
Surrogate/Tracer Recovery Test
Lead Carrier
Barium Carrier
Notes:
GFPC, Pb210, Solid "As Received"
GFPC, Total Alpha Radium, solid "As Received"
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
Page 15 of 19
uCi/kg BXFI 08/01113 1651 1310699
uCi/kg BXF I 07/26113 1639 1310694 2
Date Time Prep Batch
1359 1 310:~20;c;7;----------06124113
Anal st Comments
Result Nominal Recovery% ~----~~~~~
Ill
78,6
Acceptable Limits
(25%-125%)
(25%-125%)
GEL LA BORA TORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: August 2, 2013
Company ;
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact:
Project:
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Vegetation Analysis
North East
328139002
Vegetation
20-JUN-13 09:00
24-JUN-13
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Pb21 0, Solid "As Received"
MDC
Lead-21 0 0.000142 +/-3.68E-06 6.17E-06
GFPC, Total Alpha Radium, solid "As Received"
Total Radium 8.91 E-05 +/-2, 16E-06 I ,42E-06
The following Pre Methods were erformed:
Method Description
Dry Soil Prep Dry Soli Prep OL-RAD·A-02 1
The following Analytical Methods were performed:
Method Descri tion
DOE RP280 Modified
2 EPA 900.1 Modified
Surrogate/Tracer Recovery
Lead Carrier
Test
GFPC, Pb210, Solid "As Received"
Barium Carrier GFPC, Total Alpha Radium, solid "As Received"
Notes:
Project:
Client ID:
DNMIOOlOl
DNMIOOl
RL Units DF Analyst Date Time Batch Method ----
I,OOE-06 uCi/kg
5.00E-08 uCi/kg
·Analyst Date
CXCI --06/24113
Result
BXFI 08/01/13 1651 1310699
BXF I 07/26113 1639 1310694
Time Prep Batch
1359 1310207
A~ly~ r omments
Nominal Recovery% ----~-102
86.0
Acceptable Limits
(25%-125%)
(25%-1 25%)
2
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
Page 16 of 19
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis
Report Date: August 2, 2013
Company :
Address:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Parameter
Contact;
Project:
Client Sample ID:
SampleiD:
Matrix:
Collect Date:
Receive Date:
Collector:
Suite 600
Lakewood, Colorado 80228
Ms. Kathy Weinel
Vegetation Analysis
South West
328139003
Vegetation
20-JUN-13 08:30
24-JUN-13
Client
Qualifier Result Uncertainty
Rad Gas Flow Proportional Counting
GFPC, Pb210, Solid "As Received"
MDC
Lead-210 6.71E-05 +/-2 93E-06 6 24E-06
GFPC, Total Alpha Radium, solid "As Received"
TotalRadium 1.51E-05 +/-1.06E-06 1.96E-06
The following Prep Methods were perform."'ec.:dc.c.: ---------
RL
l OOE-06
5 OOE-08
Method Description Analyst
Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCl
The following Analytical Methods were performed: -----------Method DescriRtion
DOE RP280 Modified
2 EPA 900 I Modified
Test Surrogate/Tracer Recovery
Lead Carrier GFPC, Pb210, Solid "As Received"
Barium Carrier GFPC, Total Alpha Radium, solid "As Received"
Notes:
Counting Uncertainty is calculated at the 68% confidence level (1-sigma).
Page 17 of 19
Project:
Client ID:
DNMIOOlOl
DNMIOOl
Units OF Analyst Date Time Batch Method
uCi/kg
uCi/kg
Date
06/24113
Result
BXF I 08/01113 1651 1310699
BXF1 07/26113 1639 1310694
Time Prep Batch
1359 1310207
Anal st Comments
Nominal Recovery%
925
73.1
Acct':ptable Limits
(25%-125%)
(25%-125%)
2
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407-[phone] -www.gel.com
QC Summary
Contact:
Workorder:
Energy Fuels Resources (USA), Inc.
225 Union Boulevard
Suite 600
Lakewood, Colorado
Ms. Kathy Weinel
328139
Parmname NOM Sample Qual QC
Rad Gas Flow
Batch 1310694
QC1202899157 328139002 DUP
Total Radium 8.91E-05
Uncertainty +/-2.16£-06
QC1202899159 LCS
Total Radium 0.0013
Uncertainty
QC1202899156 MB
Total Radium u
Uncertainty
QC1202899158 328139002 MS
Total Radium 0.00212 8.91E-05
Uncertainty +/-2.16£-06
Batch 1310699
QC1202899167 328139002 DUP
Lead-210 0.000142
Uncertainty +/-3.68£-06
QC1202899169 LCS
Lead-210 0.0526
Uncertainty
QC1202899166 MB
Lead-210 u
Uncertainty
QC1202899168 328139002 MS
Lead-210 0.0854 0.000142
Uncertainty +/-3.68£-06
Notes:
Counting Uncertainty is calculated at the 68% confidence level (!-sigma).
The Qualifiers in this report are defined as follows:
**
<
>
Analyte is a surrogate compound
Result is less than value reported
Result is greater than value reported
The TIC is a suspected aldol-condensation product
9.03E-05
+/-2.16E-06
0.0016
+/-2.24£-05
4.89E-07
+/-3.18£-07
0.00223
+/-3.17£-05
0.00012
+/-4.05£-06
0.0518
+/-0.00014
-7.08£-07
+/-l.05E-06
0.0832
+/-0.000223
Units
uCi/kg
uCilkg
uCilkg
uCi/kg
uCilkg
uCi/kg
uCilkg
uCi/kg
RPD%
1.29
17.3
A
B
BD
c
D
F
H
For General Chemistry and Organic analysis the target analyte was detected in the associated blank.
Results are either below the MDC or tracer recovery is low
Analyte has been confirmed by GC/MS analysis
Results are reported from a diluted aliquot of the sample
Estimated Value
Analytical holding time was exceeded
Page 18 of 19
Reoort Date: August 2, 2013
REC% Ran e Anlst
(0%-20%) BXF1
123 (75%-125%)
101 (75%-125%)
(0%-20%) BXF1
98.5 (75%-125%)
97.2 (75%-125%)
Page 1 of 2
Date Time
07/26/13 16:40
07/26113 16:40
07/26/13 16:40
07/26/13 16:40
08/01/13 16:51
08/01/13 16:51
08/01/13 16:51
08/01/13 16:51
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 -[phone] -www.gel.com
QC Summary
Workordcr: 328139
Parmnamc NOM SamJ.!Ie Qual QC Units RPD%
K Analyte present. Reported value may be biased high. Actual value is expected to be lower.
L Analyte present. Reported value may be biased low. Actual value is expected to be higher.
M M if above MDC and less than LLD
M Matrix Related Failure
N/A RPD or %Recovery limits do not apply.
See case narrative
Analyte concentration is not detected above the detection limit
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
One or more quality control criteria have not been met. Refer to the applicable narrative orDER.
Sample results are rejected
Analyte was analyzed for, but not detected above the CRDL.
Gamma Spectroscopy--Uncertain identification
Gamma Spectroscopy--Uncertain identification
REC%
Page 2 of 2
RanJ?;e -'A:..::..:.:n.:.:ls""t--=Do..:a~te Time
Nl
ND
NJ
Q
R
u
UI
UJ
UL
X
y
Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
1\
h
QC Samples were not spiked with this compound
RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
Preparation or preservation holding time was exceeded
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more.
1\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +I-the
RL is used to evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SOIL T results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
Page 19 of 19
ATTACHMENTG
STACK SAMPLE LABORATORY RESULTS
FIRST QUARTER
RADIONUCLIDE EMISSIONS TEST
CONDUCTED FOR
ENERGY FUELS RESOURCES, BLANDING, UTAH
Prepared for:
Energy Fuels Resources
6425 S Hwy 91
Blanding, Utah 84511
Date of Report:
May 1, 2013
SOUTH YELLOW CAKE SCRUBBER
YELLOW CAKE DRYER BAGHOUSE
April 3-4, 2013
by:
TETCO
391 East 620 South
American Fork, UT 84003
Phone [phone]
Fax [phone] fax
CERTIFICATION OF REPORT INTEGRITY
Technical Emissions Testing Company (TETCO) certifies that this report represents the truth as
well as can be derived by the methods employed. Every effort was made to obtain accurate and
representative data and to comply with procedures set forth in the Federal Register.
Dean Kitchen
Reviewer: ____ _._~-~--'--v--.L-?_4----_:::; __ _
Date: _______ ~_-....:.../_--~.f--=;=,.../ ___ _
Mike McNamara Reviewer:--~~-'1/J~_,fi'----'-_/--___ _
Date: ___ .S:T--(_z.._(-"----1') _______ _
ii
TABLE OF CONTENTS
Introduction
Test Purpose ............................................................ 1
Test Location and Type of Process .......................................... 1
Test Dates ............................................................. 1
Pollutants Tested and Methods Applied ...................................... 1
Test Participants .......................................................... 2
Deviations From EPA Methods ............................................. 2
Quality Assurance ....................................................... 2
Summary of Results
Emission Results ........................................................ 3
Process Data ............................................................ 3
Description of Collected Samples ........................................... 3
Discussion of Errors or Irregularities ......................................... 3
Percent Isokinetics ....................................................... 4
Source Operation
Process Control Devices Operation .......................................... 5
Process Representativeness ................................................. 5
Sampling and Analysis Procedures
Sampling Port Location ................................................... 6
Sampling Point Location .................................................. 6
Sampling Train Description ................................................ 6
Sampling and Analytical Procedures ......................................... 7
Quality Assurance .............................. ., ........................ 7
Appendices
A: Complete Results and Sample Calculations
B: Raw Field Data
C: Laboratory Data and Chain of Custody
D: Raw Production Data
E: Calibration Procedures and Results
F: Related Correspondence
iii
LIST OF TABLES
Table
I Measured Radionuclide Emissions .......................................... 3
II Percent Isokinetics ....................................................... 4
III Sampling Point Location .................................................. 6
IV Complete Results, South Yell ow Cake Scrubber ...................... Appendix A
V Complete Results, Yell ow Cake Dryer Baghouse ...................... Appendix A
LIST OF FIGURES
Figure
1 Facility Schematic Representation South Yellow Cake Scrubber .......... Appendix D
2 Facility Schematic Representation Yellow Cake Dryer Baghouse ......... Appendix D
3 Schematic of Method 5/114 Sampling Train .................... , .•... Appendix E
iv
INTRODUCTION
Test Purpose
This test project was conducted to determine the total radionuclide emissions from the South
Yell ow Cake Scrubber and Yell ow Cake Dryer Baghouse exhausts in terms of Curies per dry
standard cubic foot (Ci/dscf).
These tests were for U-Nat on the South Yellow Cake Scrubber and Yellow Cake Dryer
Baghouse.
Test Location and Type of Process
Energy Fuels Resources is located about 5 miles south of Blanding, Utah. Uranium ore is
processed into yellow cake, which is shipped to other facilities for additional processing. There
are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the
Dryer Baghouse. The Packaging enclosure also discharges into the Dryer Baghouse. The South
Yellow Cake (SYC) dryer was the only operating dryer at the time of the test. The North Yell ow
Cake Dryer was not operating at the time of the test.
Stack schematics are shown as Figures land 2in Appendix D.
Test Dates
The first test run on the SYC Scrubber was completed April 3, 2013. The second runs was
completed April4, 2013.
One test run was completed on the Yellow Cake Dryer Baghouse April4, 2013.
Pollutants Tested and Methods Applied
The tests were a determination ofradionuclide emissions in accordance with EPA Method 5/114.
Test run filters and front wash residues were sent to Test America located in Richland,
Washington for radionuclide analysis.
Test Participants
Test Facility
State Agency
TETCO
Garren Palmer
None
Doug Olsen
Jeff Graton
Deviations From EPA Methods
None
Quality Assurance
Mike McNamara
Testing procedures and sample recovery techniques were according to those outlined in the
Federal Register and the Quality Assurance Handbook for Air Pollution Measurement Systems.
2
SUMMARY OF RESULTS
Emission Results
Table I presents the findings of the test in Curies per dry standard cubic foot. Tables IV-VII in
Appendix A have more detailed information.
Table I. Measured Radionudide Emissions
South Yell ow Cake Yell ow Cake Dryer
Run# Scrubber Baghouse
pCi/dscf pCi/hr pCi/dscf pCi/hr
1 83.2 9.384E+06 1112.3 2.26E+08
2 80.8 9.225E+06 I 'I 1[1
82.0 9.30E+06 1112.3 2.26E+08
Process Data
The process was operated according to standard procedures. All pertinent process data was
available for recording by agency personnel. Scrubber water flow, pressure drop readings (~p)
were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (~p)
were recorded and are found on the test run sheets. Production data is retrained by Energy Fuels
Resources.
Description of Collected Samples
The test filters for the South Yell ow Cake Scrubber were heavily covered with an off-white
colored particulate. The front washes were clear in appearance.
The test filters for the Yellow Cake Dryer Baghouse were lightly colored with a tan colored
particulate. The front wash was clear in appearance.
Discussion of Errors or Irre~:ularities
The South Yellow Cake Scrubber (SYC) samples were mistakenly identified on the Chain of
Custody as "NYC". Because of this mistake, the laboratory results are also marked as NYC. All
3
sampling during this test project occurred on the SYC and the Dryer Baghouse, and there was not
any sampling on the NYC.
Percent Isokinetic Sampling
Each of the tests were isokinetic within the ± 10% of 1 00% criterion specified in the Federal
Register. They also meet the Utah State Department of Environmental Quality, Division of Air
Quality specification of isokinetic sampling point by point. Isokinetic values for each test run are
presented in Table II.
Ta.b1e.II Pe.rcent lsokinetic Samnlinf!
South Yell ow Yellow Cake
Run# Cake Scrubber Dryer Baghouse
1 101 101
2 99 1:1 l [:1 •
4
SOURCE OPERATION
Process Control Devices Operation
All process control devices were operated normally. Recorded scrubber water flow, pressure and
baghouse ~p readings were recorded and are found on the test run sheets or in Appendix D.
Process Representativeness
The facility was operated normally. Production data was retained by Energy Fuels Resources.
5
SAMPLING AND ANALYSIS PROCEDURES
Sampling Port Location
The inside diameter of the South Yellow Cake Scrubber stack is 12.75 inches. The two, four-inch
diameter sample port are located 28.24 diameters (30 feet) downstream from the last disturbance
and 6.59 diameters (7 feet) upstream from the next disturbance. Figure 1 in Appendix Dis a
schematic of the stack.
The inside diameter ofthe Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch
diameter sample ports are located 28.38 diameters (454 inches) downstream from the last
disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port
locations are depicted in Figure 2 in Appendix D.
Samplin2 Point Location
Table III shows the distance of each sampling point from the inside wall according to EPA
Method 1. Each point is marked and identified with a wrapping of glass tape and numbered.
These points are determined by measuring the distance from the inside wall.
Table III. Samolin£rPoiot Location
Distance (inches) from Inside Wall
Sample Point SYC Scrubber Dryer Baghouse
1 0.85 0.70
2 3.19 2.34
3 9.56 4.74
4 11.90 11.26
5 ll 13.66
6 • I 15.30
Sampling Train Description
To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-5/114
were followed.
All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent
interference of the sampled gas and particulate.
6
The stack analyzers used to conduct Methods 1-51114 are constructed to meet the specifications
outlined in the CFR. The temperature sensors are K-type thermocouples. Heater, vacuum and
pitot line connections have been designed to be interchangeable with all units used by the tester.
A 316 stainless steel probe liner was used for the tests. Figure 4 in Appendix E is a sketch of the
Methods 5/114 sampling train.
Sample boxes were prepared for testing by following the prescribed procedures outlined in
Methods 5/114.
SampliD!" and Analytical Procedures
All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A,
Methods 5/114.
Quality Assurance
All equipment set-up, sampling procedures, sample recovery and equipment calibrations were
carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance
Handbook for Air Pollution Measurement Systems.
7
APPENDIX
A: Complete Results and Sample Calculations
B: Raw Field Data
C: Laboratory Data and Chain of Custody
D: Raw Production Data
E: Calibration Procedures and Results
F: Related Correspondence
8
APPENDIX A
Table IV Complete Results, South Yell ow Cake Scrubber
Table V Complete Results, Yell ow Cake Dryer Baghouse
Nomenclature
Sample Equations
A
TABLE IV SYC Scrubber
COMPLETE RESULTS
Energy Fuels CORPORATION, BLANDING, UTAH
SOUTH YELLOWCAKE SCRUBBER EXHAUST
Symbol DescriEtion Dimensions Run#1 Run#2
Date 4/3/13 4/4/13
Filter# X098 X099
Begin Time Test Began 7:47 7:34
End Time Test Ended 15:51 15:37
Pbm Meter Barometric Pressure In Hg Abs 24.50 24.55
~H Orifice Pressure Drop In H20 1.153 1.133
y Meter Calibration Y Factor dimension1ess 1.001 1.001
Vm Volume Gas Sampled--Meter Conditions cf 353.940 348.645
Tm Avg Meter Temperature OF 88.2 86.4
...JM Sq Root Velocity Head Rootln H20 0.7627 0.7748
Wtwc Weight Water Collected Grams 371.5 387.9
Tt Duration of Test Minutes 480 480
cp Pitot Tube Coefficient Dimensionless 0.84 0.84
Dn Nozzle Diameter Inches 0.2240 0.2240
C02 V olwne % Carbon Dioxide Percent 1.80 2.00
02 Volume% O>.)lgen Percent 17.20 17.20
N2 &CO Volume % Nitrogen and Carbon Monoxide Percent 81.00 80.80
Vmstd Volume Gas Sampled (Standard) dscf 280.391 277.653
Vw V olurne Water Vapor scf 17.516 18.289
B W s (measured) Fraction H20 in Stack Gas (Measured) Fraction 0.059 0.062
Bws (saturated) Fraction H20 in Stack Gas (Saturated) Fraction 0.110 0.119
Bws Fraction H20 in Stack Gas * Fraction 0.059 0.062
xd Fraction of Dry Gas Fraction 0.941 0.938
Md Molecular Wt. Dry Gas lb/lbmol 28.98 29.01
Ms Molecular Wt. Stack Gas lb/lbmol 28.33 28.33
%1 Percent Isokinetic Percent 100.8 98.7 AVG
Ts Avg Stack Temperature OF 111.2 113.8 112.5
As Stack Cross Sectional Area Sq. Ft. 0.887 0.887
PG Stack Static Pressure In H20 -0.750 -0.750
PbP Sample Port Barometric Pressure In_ Hg Abs 24.43 24.48
Ps Stack Pressure In Hg Abs 24.375 24.425
Qs Stack Gas Volumetric Flow Rate (Std) dscfin 1.88E+03 1.90E+03 1.89E+03
Qa Stack Gas Volumetric Flow Rate (Actual) cfin 2.65E+03 2.70E+03 2.67E+03
vs Velocity of Stack Gas fPm 2.99E+03 3.04E+03 3.01E+03
Curies Radionuclides per sample pCi 23321.0 22448.0
Crad Concentration ofRadionuclides pCildscf 83.173 80.849 82.011
ERrad Emission Rate ofRadionuclides pCi/hr 9.377E+06 9.219E+06 9.298E+06
* If the measured moisture content is greater than the saturated moisture level (supersaturated),
the saturated moisture value will be used in all calculations (40 CFR 60, Method 4, Section 12.1.7)
Dryer Baghouse
TABLEV
COMPLETE RESULTS, PM
DENISON MINES CORPORATION
YELLOW CAKE DRYER BAGHOUSE
Symbol DescriEtion Dimensions Run#!
Date Date 4/4/13
Filter# XlOO
Begin Time Test Began 9:50
End Time Test Ended II :54
Pbm Meter Barometric Pressure In. Hg. Abs 24.55
~H Orifice Pressure Drop In. H20 1.594
y Meter Calibration Y Factor dimensionless 1.004
Vm Volume Gas Sampled--Meter Conditions cf 96.458
Tm Avg Meter Temperature OF 76.8
;j~p Sq Root Velocity Head Root In. H20 0.8216
Wiwc Weight Water Collected Grams 10.4
Tt Duration of Test Minutes 120
cp Pitot Tube Coefficient Dimensionless 0.84
Dn Nozzle Diameter Inches 0 .2215
C02 Volume %Carbon Dioxide Percent 0.00
02 Volume% Oxygen Percent 20.90
N 2 &CO Volwne %Nitrogen and Carbon Monoxide Percent 79.10
Vmstd Volume Gas Sampled (Standard) dscf 78.5 33
Vw Volume Water Vapor scf 0.490
Bw5 Fraction H20 in Stack Gas Fraction 0.006
xd Fraction of Dry Gas Fraction 0 .994
Mct Molecular Wt, Dry Gas lbllbmol 28.84
Ms Molecular Wt. Stack Gas lbllbmol 28.77
%1 Percent Isokinetic Percent 100.8
Ts Avg Stack Temperature OF 96.3
As Stack Cross Sectional Area Sq. Ft, 1.396
Po Stack Static Pressure In.H,_O -0.41
PbP Sample Port Barometric Pressure In. Hg Abs 24.48
Ps Stack Pressure In. Hg. Abs 24.450
Q, Stack Gas Volumetric Flow Rate (Std) dscfin 3.39E+03
Q. Stack Gas Volumetric Flow Rate (Actual) cfin 4.39E+03
vs Velocity of Stack Gas fjJtn 3.15E+03
Curies Radionuclides per sample pCi 87350.0
Crad Concentration of Radionuclides pCildscf 1112.2698
ERr ad Emission Rate ofRadionuclides pCi/hr 2.261E+08
General Nomenclature
%1 = percent isokinetic, percent
As= (D/ I 4) • 1t
ASM> = see '>/!'J.P
Btu= unit heat value (British thermal unit)
Bws = fraction of water in stack gas (may have designation of "measured" or "saturated")
"measured" represents measured moisture based upon sample volume and water collected
"saturated" is a calculated value based upon stack pressure and temperature
C0 = average of initial and final system zero gas calibration bias checks (ppm, percent)
Cavg = average gas concentration (as measured)
C8 = concentration of particulate matter, back half (gr/dscf,lb/dscf, etc.)
ccond = concentration of condensibles (grain/dscf)
Ccors = concentration of coarse particulate (gr/dscf)
Cnir = measured concentration of a calibration gas when introduced in direct calibration mode
Cra = concentration of particulate matter, front half, actual stack flow (gr /acf)
CF = concentration of particulate matter, front half (gr/dscf,lb/dscf, etc.)
Cgas = Cavg corrected for initial and final system bias checks (Equation 7E-5)
Cm = average of initial and final system upscale gas calibration bias checks (ppm, percent)
Cma = actual concentration of upscale calibration gas
Cmetal = concentration of metals (ppm, J..Lg/fe, etc.) atomic symbol replaces "metal"
C02 = percent carbon dioxide in the stack gas
cp = pitot tube coefficient (0.84)
CPMJO = concentration ofPM10 particulate (gr/dscf)
Crad =concentration ofradionuclides (pCildscf)
CS = measured concentration of a calibration gas when introduced in system calibration mode
Cx = Any species symbol may replace X. Units may be expressed as ppm, lb/dscf, etc.
Cx (corr) = actual gas concentration corrected to required percent 0 2
Curies = Measured radionuclides per sample. Units may be pCi or uCi.
De= jet diameter (em)
DIF = Dioxins and Furans (See laboratory report for D/F descriptions and nomenclacture)
!'J.H = orifice pressure drop (inches H20)
!'J.H@ = orifice pressure (inches H20)
!'J.Hd = orifice pressure head (inches H20) needed for impactor flow rate
Dn = nozzle diameter (inches)
!'J.P = stack flow pressure differential (inches H20)
Dp50 = 50% effective cutoff diameter of particle (em)
Ds = diameter of the stack (feet)
EA = percent excess air
ER8 = emission rate of back half particulate (lb/hr)
ERcond = emission rate of condensibles (lb/hr)
ERcors = emission rate of coarse particulate (lb/hr)
ERF = emission rate of front half particulate (lb/hr)
ERgas = emission rate of a gas (lb/hr)
ERmmBtu = emission rate per mmBtu of fuel
ERPMJO = emission rate ofPM10 particulate (lb/hr)
ER,ad =emission rate ofradionuclides (pCi/hr)
ERx = emission rate of compound which replaces X. Units are usually in lb/hr.
Fn = Dry based fuel factor. Ratio of the gas volume of the products of combustion to the heat content
See 40 CFR 60, Appendix A, Method 19, Table 19-2 for fuel factor values.
Kc = Cunningham slip correction factor
'A= mean free path of molecules in gas phase (em)
mmBtu = million Btu
General Nomenclature
Mcond = mass of condensibles (milligrams)
Mcors = mass of coarse particulate (milligrams)
Md = molecular weight of stack gas, dry basis (lb/lb-mol)
MF = mass of particulate on filter (mg)
MFP = mass of particulate matter on filter and probe (mg)
mmBtu = million Btu
Mp = mass of particulate matter in probe and front wash (mg)
MPMIO = mass ofPM10 particulate (milligrams)
M5 = molecular weight of stack gas, wet basis (lb/lbmol)
Mx = mass of species "X". Units may vary and other descriptive subscripts may apply.
lls = gas viscosity (poise)
Mwx = molecular weight of gas species (g/gmol)
N = number of jets per plate
N2 = percent nitrogen in the stack gas
0 2 = percent oxygen in the stack gas
'1/t:,p = average of the square roots of L'lP (may also be referred to as ASL'lP)
'l/t:,p1 = square root of L'1P at point I of the current test, Method 201A
'l/t;P1' = square root of L'lP at point 1 of the previous traverse, Method 201A
'1/t:,p'ave = average of the square roots of L'lP from the previous traverse, Method 201A
Pbm = absolute barometric pressure at the dry gas meter (inches Hg)
PbP = absolute barometric pressure at the sample location (inches Hg)
PG = stack static pressure (inches H20)
P5 = absolute stack pressure (inches Hg)
Pstd = absolute pressure at standard conditions (29.92 inches Hg.)
e = time of test (minutes)
81 = sample time (duration in minutes) at first sample point for Method 201A
en= sample time (duration in minutes) at sample point "n" for Method 201A
81est~ target test time for Method 201A (minutes)
Oa = stack gas volumetric flow rate (acfm)
Os = stack gas volumetric flow rate (dscfm)
Osc = actual gas flow rate through the cyclone (acfm)
Osee = actual gas flow rate through the impactor (acfm)
Ow= wet stack gas std. volumetric flow (fe/min, wscfm)
R = gas constant (21.85 inches Hg*fe /(lbmol*R))
Pp = particle density (1 g/cm3)
Ps = stack gas density (g/cm3)
T m = stack temperature (°F)
T5 = stack temperature (°F)
Tstd = absolute temperature at standard conditions (528°R)
Tt = Duration of test run in minutes. Also see 8
Um = mean molecular speed (cm/s)
Vm = sample volume (fe) at meter conditions
Vmstd = volume standard (dscf), sample volume adjusted to 68°F and 29.92 inches Hg.
V s = velocity of stack gas ( fpm)
V w = volume water vapor (sci) at 68°F and 29.92 inches Hg.
W!wc = weight of the condensed water collected (grams)
xd = fraction of dry gas
Y = meter calibration Y-factor (dimensionless)
\jl = dimensionless inertial impaction parameter, 0.14
General Sample Equations
%1 = Vmstct • (Ts + 460) • I039 I (8 • Ys • Ps • Xd • Dn2)
As= (D/ I 4) • 1t
Bws = V w I (Vmstd +V w)
CB = MB • O.OI543 I Vmstd
Cconct = Mcond • O.OI543 I Vmstd
Ccors = Mcors • O.OI543 I Vmstd
Cra = Tstct • Cfp • Ps • Xct I [Pstct • (T m + 460)]
Cr= Mfp • O.OI543 I Vmstd
CPMIO = MpM1o • O.OI543 I Vmstd
Crad = CuriesiVmstd
Cgas (corr) = Cgas • (20.9 -desired %02) I (20.9 -actual %02)
case Dpso = -..J [J-lS • \jf • N • 1t • D/ • I8 I (Kc • Pp • Qsce • 4)]
I 0,2091 0 7091
PM, DPso = O.I5625 • [(Ts + 460) (Ms • Ps)] • (1-ls I Qsc)
ERcond = Ccond • Qs • 0.00857
ERcors = Ccors • Qs • 0.00857
ERF = Cr • Qs • 0.00857
6 ERgas = Pstd • Qs • Mwgas • Cgas • 60 I (R • Tstd • IO )
ERgas = Cgas(lb/dscf) • Qs • 60
(Either ERgas equation gives equivalent lblhr values to 3 sig. figures)
ERmmBtu = Cgas(lb/dscf) • Fd • (20.91(20.9-%02), Method I9 Equation I9-I
ERPMIO = CPMIO • Qs • 0.00857
ERrad = Crad • Qs • 60
Kc = I + 2 • A • I.257 I Dp5o
A = 1-ls I (0.499 • Ps • U m)
Mct = C02 • 0.44 + 0 2 • 0.32 + N2 •0.28
Ms = (Mct • Xct) + (I8 • Bws)
1-ls = [51.05 + 0.207 • (T, + 460) + 3.24 •10'5 • (T, + 460)2 + 0.53147 • %02-74.143 • Bwsl • 10-6
Ps = Pbp + (PG I 13.6)
81 = (-YL'lP,' I -..Jt'lP'ave) • (8test I pts)
8n = 81 • -..Jt'lPn I -..Jt'lP1
Qa = Ys • As
Qs = Qa • Xd • Ps • Tstd I [(Ts + 460) • Pstdl
Qsc = [(Ts + 460) • Pstd I (Tstd • Ps)] • [(Vmstd + Yw) I 8]
Qsce = [(Ts + 460) • Pstd I (Tstd • Ps)] • [(Vmstd + Yw) I 8]
Qw= QsiXd
Ps = Ps • Ms • 3386.39 • 10-6 I [R • (Ts + 460) /1.8]
Um = IOO • -..J {[R • (Ts + 460) I 1.8 • 8 • I03] I [n • Ms]}
Vmstd = Vm • Y • Tstd • (Pbm + t'lH I 13.6) I [Pstd • (Tm + 460)]
Ys = 85.49 • 60 • Cp • -..Jt'lP • -..J [(Ts + 460) I (Ps • M5)]
Yw= Wtwc • 0.047I5
Xct = I-Bws
APPENDIXB
South Yell ow Cake Scrubber
Preliminary Velocity Traverse and Sampling Point Location Data
Field Data Sheet
Yell ow Cake Dryer Baghouse
Preliminary Velocity Traverse and Sampling Point Location Data
Field Field Data
B
South Yell ow Cake Dryer Scrubber
Preliminary S Y Cake Serb
1
Facility Energy Fuels
Stack Identification South Yell ow Cake Dryer Scrubber
J! Date !-L~7r( l
N Barometric Pressure
Pbm in Hg Pbr in Hg
---i B Static Pressure (P 0) in H20
Estimated Moisture (Bw,) 4-6 %
Sample Height from Ground 70 feet
Comments:
Stack Dia. 12.75" Reference: 0"
Ports are 7' Upstream from next disturbance
Ports are 30' Downstream from la~t disturbance
Traverse Percent Distance From: Ports
Point Diameter ID Reference A B c D E F
1 6.7 0.85 0.85 ,.~ .r5 I 11/ .s-o
2 25.0 3.19 3.19 Jl), /d' ·s-e, .c1"
3 75.0 9.56 9.56 IO "F I c)" -t..l • "'Cj(
4 93.3 11.90 11.90 /D" .vv to~ . u ':>
Averages:
Ts ___ _ L.Flow ----
~P ___ _ -J~p ----
KEY=> ~..IT_s __ ....;M=-_L._F_l_ow_.l
----Field Data Sheet Page _l_of+ Run# __ l_
Plant: En.emv eyu.~s -----------
Date:/d /--.J ~ f 3 _
Traveru II Ti~e ~ AP II AH <;nH,O) II Vacuum II 1 Te":peratures :""' 1 II DGM T?"p IT~l DGM
Point Clock I Min (e) II <~'l II <"' 11.01 U Desired I Actual II tin"'' II Stack (1,) I Probe I Probe out I Oven l Emuent U Out I In
I .() N
1 0
1 Z. 0 Stack Diameter 12.75" Port Reference_Ol!..."--
1 \f 0 Ports are 7' Upstream from next disturbance
2 b 0 Ports·are 30' Dovmslream from IBn disturbance
2 '1-D Assumed Moisture 4-6 %
2 1.0() Probe "2 * Cp 0.84
3 (1,D
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Average -,~ _ -:tlr-vl-t. \G' 3 .g-g-. 0
Additional (Extra) Leak Check Information
I I DGM before Leak Check I Vac f'Hg) I Rate (ft~/min) II DGM After Leak Check I Vac ("Hf1) I
Noik: 3alibrat~o.!' . l .) ..f , t ·~ .vz-\ .~
Avg Q. • Z. ~~ i.:;;;----
Gas Bag_ f{-y)
Console 5-"
Y-Factor / ·Oo} AH®~inH10
Barometric Pressures
Pbm_ -'1 . .'·(.')0 __ in Hg
P>, l~q--inHg
1'0 l f ~ inH10
Lealc Check: Pre fllli, -z
A'lmon 0. O.D & .o-oO 7
vac!nHg-'2-l ·-• fz_
---l
Pi tot Rotc {)-Q -·-..t..
lnH,O -?1 :L
Water Collected
Time Sampled_
Review
K=
Ko:
Rate (ft,/min)
()·()
~
J 7;,r s
'( &-0 min (L
I
@T ...
@Tm
6y-; . v\ '7l~ ~~~Dam Sheet
Plant Ene~y F~~s\
Date:_ '{:;-\ j.')
Point
Traverse~~ Time I
Clock 1 Min (6)!
DGM
(ft.')
~ETCO ?
FilterL 'f.Jt5!-/ Sample Box_k-Page _\_of-+-Run #. Z-
Location: SouYQ'ello~ake Dryer Scrubber
Operator: -tL.-;L=\-------, . rt
In
AP II AH ';""""~ Jl Vacuum~ 1 Te~peratures ~71 1 II DQ~ T~p(T.J
'"' lttl 11 Stack (T ,) I Probe I Pro~ out I Oven '"' ""'' II Desired I Actual Effluent H Out
I 86 N
Stack Diameter 12.75" Port Reference_O,_" __
1
2
2
2
3
3
3
4
4
4
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-; -2Y '6 -v ~ s--J \ ~--s-1<~ r-t 1 t ~ -1.:1-s -t "' t L( 1 ·· Total
7' Upstream from next disturbance
30' Downsueam from last distutbance
Assumed Moisture 4-6 %
Probe Z 1{p Cp 0.84
~~~re jalibmtio:'. 1 . ..) ..f
, t -~ -~\ .'Zk
AvgD~ • ZP"'I in~ --
~Bag (.;-o 3
Console--::::-
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BaromwicPressu~
Pb., •. -z_'t.{: --y-2.._ in Hg
Pb0_ Z ~ · t.f I{ ~\l Hg PG-ce ·1-~ nH20
Leak Check: Pre ('/ ~
ft'Jmin · D .QO ~ · c? .oo"l
Y3C i• Hs-'1.-r--:· r -z..--
Pitot Rote 0 · 0 - _ ... ...G._.,..-
lnH,O q. £_
Q·O
~
Water Collected '"3 & 1 J .g
Time Sampled_ r'!?J 1 min
Review
l
!Average v.r1-~~ t-\7) ~\)·S g~.~ ~= =~=
AdditionaiLExtra) Leak Check Information
DGM before Leak Check Vac ("Hg) Rate (tetmin) DGM After Leak Check Vac ("Hg) Rate (termin)
Yell ow Cake Dryer Baghouse
Prelim 6 pts blank
i
Facility Energy Fuels Resources, Blanding, UT
Stack Identification North Yellow Cake Dryer Baghousc
Date Y/4/1)
i Barometric Pressure
B Pbm 2,~,,-).....-in Hg PbP l~ .~f2 inHg
N 0 Static Pressure (P 0) ..... II inHP
A Estimated Moisture (Bw,) I %
Sample Height from Ground feet
Comments:
Stack Dia. 16 Reference: 0
Ports are 57" Upstream from next disturbance
Ports are 468" DO\mstrcam from last disturbance
Traverse Percent Distance From: Ports
Point Diameter ID Reference A B c D E F
I 4.4 0.70 0.70 e+ 4i
2 14.6 2.34 2.34
3 29.6 4.74 4.74
4 70.4 11.26 11.26 'II ta-
5 85.4 13.66 13.66
6 95.6 15.30 15.30 'fZ. "7,.
~
1
l
l
Averages:
Ts LF!ow ----
t.P .YM' --------
KEY==>
~
slit«-{ TETCO ,-
Filter).( (tOO Sample Box_L Field Dato Sheet Page _t_of_l_ Run#_\_
Plant: Energy Fuels Resources. 131anding. UT
Date: 'i/ "f.( 13
Traverse Time DGM 6P
Point Clock Min(8) (0'') t'tl11j0l
1 q·.it) 0 '-4'11 Z..{l-..... 4
2 10 ~~7.ol1o .,-)
3 l.O ~{j.~:{ • c., -:r-
4 30 ~.t>C{.•.no . ~l.
5 ~0 '-ti..~.L'Z-0 ·S3
6 so '( 1-l.. .~00 ·So
1 rv ;5~ bO '-IS) .. •Ob •'1T'
2 10 I.{ 't ~· o(,o . •81
3 Bo Sol. ~~o ·8o
4 90 511.4~1 .e~
5 loo .$1.0. ~95' •18
6 110 's'"lc:l\. DO •ll
u:s~.~ ~20 5 Y?-.110
-------
6H (nH,Ol V1cuum
Desired Actual (11111!!11
·1S .16 1...
114. L~lf L
L -{;) L{J '-i
I , ~B_ 1.~12_ 'l
l· ~ I·~ y
I· 9l-I.~L ~
'.-? \ \.ll <-\
to01./ l.46<f y
1-~'2. t.B~ q
l.oo z.o_o~ .. ,
loll 1.11 ...
t."7-s' I • I'> '{
Total 9(,.y~s ,.,,.<oS'tl../ \'Lr~v
-,J ' ~'L\~ \ . 5~1{ Avera~
Comments: Time Baghouse 1\P Time Bagh0~111\P
(O•.Q_~ (.,_.1, ~r.o) e./
!().I.( 1.\ r1. •. t.{ 11.o
i\1 ~4{ <6·?... \(.'.•\\ ~--
Location: North Yellowcake Dryer Baghouse
Operator:~ I &e M. A !;;,.tf~(o-
Temperatures m DGM T~rll? (T.)
Stack (T,) Probe ProbeOui Filter Emuent Out In
'i:> L~~~ l."'3 z.c. ·~ 5'2.-t,.-4 (,f
9~ J_{.,\o l.C.~ t<. J ~4cl t..B ~:3
'1{p 'l-3o £.(.,( ~~.., 'n ,.-) ~3
'f(c 2. 70 l->1 l-.-1 Lf) 6o b )
'11o l<..( I.') '-t . ~l't 'i1-103 bS
'1(D L31 l;'i Z-l'f 4'f 'iH· :=jl-(
.,~ 2.5"3 2-5'"0 z.ra So 8:( T~
'1t.. lG.fo lt,O 2.(,0 5'-l ~§ 1-(
Cj<.. Z.3Q l<~ l,-)) 55 ~0 TI
<1':1-lCi-) 2\'1 U'1 5-r q\0 1J?
~B Lio z. "'{ l(,<{ 5R Cf·j 1~
9S l.S3 l-5''1 'U<i .'1'9 ~I 1_8_
------_I_ -\
1\SCv../ 18 q)V'
9~·) -l~·~ ~ .
i B A() N
Stack Diameter _16" __ Port Reference _o,o·_
Ports are
Ports are
~Upstream from next disturbance
468" Downstream from last disturbance
Assumed Moisture _ __.:.. __ %
Probe U1.!t Cp~
Nozzle Calibration
• it. I 1 tz.l o l,l z_ I Z.l. Z.
~--­
Avg 0, • Z. Z. I l inches
Gas Bag Ambient Air
Console ~"f
Y-Factor (.oo'-1
. hH0 t . (.. 1 q in H,O
[3arometric Pressu,!Ss
Pb •• z<{,j) inHg
Pb0 Z. '{ • '"I B in Hg
P0 -I ~-.•ll in H10
Le1k Chcd. Pre
f.'lmin O·COZ,
""'inHs 'Z. 2·'0
Post
~
~
Pi!OI Rale 0·0 ___.2:_Q
· .. , !!. H,O g ·0 ___l:_Q.
Water Collected I 0 • '-{ g
Time Sampled \ '2.0 min
Review (lii.JJL4.
K= @Tm
K~ @T. ..
1 [,o~IJ-t-\'> r,~ee7P ~
South Yell ow Cake Scrubber
Sample Recovery
Gas Analysis Data (ORSAT)
Yell ow Cake Dryer Baghouse
Sample Recovery
Gas Analysis Data (Ambient)
Chain of Custody
Lab Analysis
APPENDIXC
c
South Yell ow Cake Dryer Scrubber
METHOD 5
Facility: Denison Mine
Stack Identification: NYC Scrubber ~~~~~-------------------------
Date: ------------
IMPINGERS
Run: Sample Box: ()
1Dlp1nger Number
1 2 6
drop out
Final (gl S':j.Z ·
Initial (g) _c.!..:( ~::i-1·_,.1:=+. ~rt-~""7'""~~-:--::,.r-,,......_..L-.-,:iM~~--~...:.._+-:.._--'----r
N et (g) 1-:!$'f) -==~==~====~====~====~~~~~===F
Total (g)
--------IMfiNGEBS
Run: 2 Sample Box: D
X()99 Impinger !Qumlier
2 I 3 I 4 I 5 6
Initial Volume of liquid (litO) in impingers, (ml) ;2; droE out I 100 I 100 I Silica Gel
'
Final (g)
Je::,
Total (g) )s-1-!
-~·-~-... ··---IMriN~ERS
Run: Sample Box:
liiipmger rqum6er
2 I 3 I 4 I 5 6
Initial V11!umt of I quid ~120) in impingurs, (ml)
drop out I 100 I 100 I Silica Gel
'
Final (g)
Initial (g)
Net (g)
Total (g)
IMPI~~ERS
Run: Sample Box:
]mptnger ~um5er
2 I 3 I 4 I 5 6 -lnitiul Volume of liquid (H20) In Jrnpingcrs. (ml),
droE out I 100 I IOO I Silica Gel
J
Final (g)
Initial (g)
Net (g)
Total (g)
Plant f~"":.L.e=Y'l=~-i=~--....:11?_.~_~_(_s _____ _ Location, __ 5_Y....~.....{_ ____________ _
Analytical Method. ___________ _
Dot' 5(( Average
Ach1al Net Actual Net Actual Net Net
Gas Reading Reading Reading Volume
Tes1No.
Gas Bag No. H--o 2 COz \ . 8" I·? {. ~ f·cS-/-g-l.g-/:r Ambienl Temp'*=-
Operator 0 2 (Net is Actual 0 2
Reading Minus Actual 1'1-t... I 7-·t.-.
Average
?./6~ Net Actual Net Actual Net Net
Date Gas Reading Reading Volume
Test No. '2-
Gas Bag No. 6-03 coz 2·0 z. c) Ambient Temp~ -z.o Z·O Z:.·O z.. c) 2·w
Operator
t-1-·1..-10-v ,-:;,~ 17-.
rr-----T------1~--~r---~~--~r---~J Avernge
Date ----Test No. ____ _
Gas Bag No.-----
Ambient Temp ____ _
Operator ____ _
Gas
Actual
Reading
Net
tol was dctennined using a gas analyzer
CO is not measured, as it has the same molecular weight as N2
Net Net
Volume
Yell ow Cake Dryer Baghouse
NYC Baghouse M5
Facility: Energy Fuels Date: '-[( !.i./13 --~~-----
Stack Identification: ..;;.N_Y_C_B;;;.....oag"--h..;..ou'-s_e ____________ _
IMPINGERS
XofOO
IMPINGERS
IMPINGERS
IMPINGERS
Final (g)
Initial (g)
Net (g)
Final (g)
Run: Sample Box:
Impmger Number
_L 2... I 3 I ....i.. I 5
Init ial Volume of liquid {H10) in impingers, (ml)
I 00 I 00 I I Silii:a <•cl I
I > I ' ;
~~lf . ~ ~40. l-5 "31.) 0'11.""1-
{pVj {;.. 7 (p~)-3 5z&. ~ <J'f5-I
-2l.<f '·'l 5.~ 2. 'l>. ~
Total (g) f 0 I '-1
Run: Sample Box:
liDpiQger Number
..L 2 . I 3 I 4 I s
lniJinl Volume of liquid (H10) in lmoingc;r ; (ml)
I 00 I 00 I I Silica Gel I
---~---~----+----r----r----
Initial (g) ___ ---1-----t----+----+----+----
Net (g) ============================================
Total (g)
Run: Sample Box:
lmpmgcr Number
..1... 2 I ...L. I 4 I s .6
Initial Volume of liquid (H20) in impingers, (ml)
100 100 I ] SilicaGel ]
Final (g) ___ ---1-----t----+----1-----+----
Initial (g) ---~-----Net (g) ======~====================================
Total (g)
Run: Sample Box:
1 -2 I 3 I 4 I s
lmfnger Number
Initial Vohrme ofliquid'(H10) in lmpingcrs,. (mil
IOO 100 I I SilicaGel I
Final (g)------1-----t----+----+----+----
Initial (g) -----1-----t----+----+----+----Net (g) ========================~====~======
Total (g)
Chain of
Custody Record
.. __ , .... ,,.,..,[
Cllsnr
Tetco --Address 391 East 620 South I_
C1ly -1.; ~z~~3 American Fork
Proloa N4m:: er-4 'l.«lJIJQ11 /Sl.!/!:1
Enern:v Fuels.2013 1st Quarter
CcnlfrJ1:t!Pumna~ OtrJotf(}(.i<:ita. Ko •.
---Sample J.D. No. and DescriptiOn Dare (Containers tor 91100 sampiQ may b9 combined on oru1line)
XlOO Rl Baghouse filte~ and beak:r. 4/4/2013 -c
X098 Rl NYC filters and beaker 4/3/2013
1 X099 R2 NYC filters and beaker ! 4/4/2013 -
'"" .....
-
Temperature on R9ce/pt ---Test America
Drinking Water? Yes 0 No 0 THE LEADER IN ENVIRONMENTAL TESTING
Prck;ct M8naqer Dale Cfri!l~ of CiJ5Wv' Nu"'tt8r.
Dean Kitchen ! 4/5/2013
TIWSI1I!or.9 Mui>!>er'lllrM Code)!Fax MJmbor LBbNurnber l t ' 801-492-9106 Psge of
S/l,.Ccr.ma I Lab Coo/act Analysis (Attach list if
scott Chrbtemen,G•rren P1lmer more soacals neooed)
C~tl•imNiityMI Number I Special InstructionS/
Containers l! 0 Conditions of Receipt Matrix Preservatives _1:;: "' ....
N 'l'
~ i "' N N ,
~ ~ ~ ~~ ~ t .. "' rme .. i ~ ~ .. _,
~ .t ' -J 9:00 .x X
) I ' 7:30 X: X I
7:30 X i j l( I
I I ' i ' I I I I I . I i !
I f
l
I I
I I
I f I
i h ,., .... _ -~' --•---·~ '(/;Qt/!icolian ~-··~--·-~-d. {A fee fTIDybe fJSS8113od ff 9Nf!pleStue re!IJirMd 0 Non·Hszard 0 F/smmabl" 0 S/cin lrrimnt 0 Poison B • 0 Unlmawrr 0 R"lum To Cliett I ""!. Dlsposar By Lab 0 An:hive Fer ___ Months lorgor v .. m t mmlh) ac: Rcouitcr;;enr.s (Sp(l:;ityJ
0 14 Oays 0 21 Days
1. Rr1c8MK1 By Trme
2. ffllee~led3y
1
O;grs jl7mo
3:R~iiiSI'C4dBy Trrne 3, Rir...IIN#d By
1
O'~re , 11me
ccmm4~1&
When Complete Email to: Dean or Paul [e-mail]
01971liBUTK>N: -Wffir~-Ref.irned f6 C/ii;nl JOilf/Riij}Q~NARY~ Slays INI"tfl rrre-sampie; r-JNJ(-F:6KrCCpy
SDGNo. Order No.
46619
TestAmerlca
rptSTLRcbTitlc v3.73
TestAmerica
Analytical Data Pacl{age Prepared For
Denison Mines (USA) Corp.
Radiochemical Analysis By
TestAmerica
2800 G. W. Way, Richland Wa, 99354, (509)-375-3131.
Assigned Laboratory Code:
Data Package Contains 15 Pages
Report No.: 55334
Results in this report relate only to the sample(s) analyzed,
Client Sample ID (LI11t Order) Lot-Sa No. Work Order Report DB ID
X098 R1 NYC filters and J3D100435-2 MOKM21M 9MOKM210
beaker
X099 R2 NYC filters and J3D100435-3 MOKM31AA 9MOKM310
beaker
X100 R1 Baghouse filter J3D1 00435-1 MOKM11AA 9MOKM110
and be
Page 1 of 15
Batch No.
3104033
3104033
3104033
I
I i
t ;
I •
..
Test America
THE LEADER IN ENVIRONMENTAL TESTING
Certificate of Analysis
April 30, 2013
Denison Mines (USA) Corp
1050 17th Street, Suite 950
Denver, CO 80265
Attention: Dean Kitchen
Date Received at Lab
Project Name
Sample Type
SDGNumber
I. Introduction
April 10,2012
Energy Fuels 20 13 1st Quarter
Three (3) Stack Filter Samples
46619
CASE NARRATIVE
On April 10, 2013, three stack filter samples were received at TestAmerica's Richland laboratory for
radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification
numbers as described on the cover page of the Analytical Data Package report form. The samples were
assigned to Lot Numbers J3Dl00435.
II. Sample Receipt
The samples were received in good condition and no anomalies were noted during check-in.
m. Analytical Results/Methodology
The analytical results for this report are presented by laboratory sample ID. Each set of data includes
sample identification information; analytical results and the appropriate associated statistical
uncertainties.
The analysis requested was:
Alpha Spectroscopy
Uranium-234, -235, -238 by method RL-ALP-004
IV. Quality Control
The analytical result for each analysis performed includes a minimum of one laboratory control sample
(LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments"
section.
TestAmerica Page 2 of 15
1
'
Denison Mines (USA) Corp
April 30, 2013
V. Comments
Alpha Spectroscopy
Uranium-234. 235, 238
The LCS, batch blank and sample results are within acceptance limits.
I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically
and for completeness, for other than the conditions detailed above. The Laboratory Manager or a
designee, as verified by the following signature has authorized release of the data contained in this hard
copy data package.
Reviewed and approved:
TestAmerica Page 3 of 15
Drinking Water Method Cross References ··----·---·· .. ·---.-----·---...... ·--__.......·~----·---
~--DRINKING WATER ASTM METHOD CROSS REFERENCES --
Referenced Method lsotope(s) TestAmerlca Richland's SOP No.
EPA901.1 Cs-134, 1-131 RL-GAM..Q01
EPA 900.0 Alpha & Beta RL-GPC-001
EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002
EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002
EPA 903.1 Ra-226 RL-RA-001
EPA 904.0 Ra-228 RL-RA-001
EPA 905.0 Sr-89/90 RL-GPC-003
ASTM D5174 Uranium RL-KPA-003
EPA 906.0 Tritium RL-LSC-005
1----· -l ·----.
I . . ... ·-. ·--··--.._ --
Results in this report relate only to the sample(s) analyzed.
Uncertainty Estimation
TestAme1·ica Richland has adopted the internationally accepted approach to estimating
uncertainties described in "NIST Technical Note 1297, 1994 Edition". The approach, "Law of Propagation
of Errors", involves the identification of all variables in an analytical method which are used to derive a
result. These variables are related to the analytical result (R) by some functional relationship, R = constants * f(x,y,z, ... ). The components (x,y,z) are evaluated to detemline their contribution to the overall method
uncertainty. The individual component uncertainties (u;) are then combined using a statistical model that
provides the most probable overall uncertainty value. All component uncertainties are categorized as type
A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the
components, such as sample homogeneity, are combined with the component uncertainty as the square root
of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result
is the combined uncertainty (u.) multiplied by the coverage factor (1,2, or 3).
When three or more sample replicates are used to derive the analytical result, the type A
uncertainty is the standard deviation of the mean value (S/? n), where S is the standard deviation of the
derived results. The type B uncertainties :are all other random or non-random components that are not
included in the standard deviation.
The derivation of the general "Law ofPwpagation of Errors" equations and specific example are
available on request.
TestAmerlca
rptGencrallnfo v3.7Z
TestAmerica Page 4 of 15
·-
..
.. ... -·--
·--
--
.
I
; '
I· Action Lev
Batch
Bias
COCNo
C()unt Error (#s)
Total Uncert (#s)
U0 ~ Combl11ed
Uncertainty.
(#s), Coverage
Factor
CRDL(RL)
Lc
Lot-Sample No
MDqMDA
Primary Detector
Ratio U-234/U-238
Rst/MDC
Rst!l'otUcert
Report DB No
RER
SDG
Sum Rpt Alpha
Spec Rst(s)
Work Order
Yield
TestAmerlca
rotGcuernllnfo vJ. 72
TestAmerica
Report Definitions
An agreed upon activity le,,elu:;cd to IHggcr some ncllon wluln the fi nal result is greater tha11 or equal to the Action
Level. Often the Action Level is rel;\ted to the Decision Limit.
The QC preparation batch number that relates laboratory samples to QC samples that were prepllfed and analyzed
together.
Defined by the equation (Result/Expected)-I as defined by ANSIN13.30.
Chain of Custody Number assigned by the Client or TestAmelica.
Poisson counting statistics of the gross sample count and background. The uncertainty is absolute. and in the same
units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background.
All known uncertainties associated with the prepllfation and analysis of the sample life propagated to give a measure
of the uncertainty associated with the result, Uc the combined uncertainty. The uncertainty is absolute and in the
same units as th~J result.
The coverage factor defines the width of the confidence interval, I, 2 or l standard deviations.
Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmerica "default"
nominal detection limit. Often referred to the t<eporting level (RL)
Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
associated with the sample. The Typ!J I error probability is approximately 5%. Lc=(1.645 •
Sqrt(2*(BkgrndCnt!BkgmdCntMin)/SCntMin)) • (ConvFcti(Eff*Yld*Abn*Vol) * lngrFct). For LSC methods the
batch blank is used as a measure ofthe background variability. Lc cannot be calculated when the background count
is zero.
The number assigned by the LIMS software to track samples received on the Sllflle day for a given client. The
sample number is a sequential number assigned to each sample in the Lot.
Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
with a Type I and II error probability of approximately 5%. MDC= (4.65 ~
Sqrt((BkgmdCnt/BkgrndCntMin)/SCntMin) + 2.71/SCntMin) * (ConvFcti(Bff • Yld • Abn *Vol)~ lngrFct). For
LSC methods the batch blank is used as a measure of the background variability.
The instrument identifier associated with the analysis of the Sllfllple aliquot.
The U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural untnium in NIST SRM 4321 Cis
1.038.
Ratio ofthe Result to the MDC. A value greater than I may indicate activity above background at a high level of
confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers
associated with the result.
Ratio of the Result to the Total UncQrtainty. If the uncertainty has a coverage factor of2 a value greater than I may
indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence
interval. Caution should be used when applying this factor and it should be used in concet1 with the qualifiers
associated with the result.
Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order
Number.
The equation Replicate Error Rntio"' (S·D)/[sqrt(TPUs2 + TPUd2)] as defined by ICPT BOA where Sis the original
sample result, D is the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is lhe
total uncertainty ofthe duplicate sample.
Sample Delivery Group Number assigned by the Client or assigned by TcstA.merica upon sample receipt.
The sum of the reported alpha spec results for tests derived from the Sllflle sample excluding duplicate result where
the results are in the same units.
The LIMS software assign test specific identifier.
The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method.
Page 5 of 15
Report No. : 55334
Client ld
Batch Work Order Parameter
3104033 FFSR
X098 R1 NYC filters and beaker
MOKM21AA U-234
U-235
U-238
X099 R2 NYC filters and beaker
MOKM31AA U-234
U-235
U-238
X100 R1 Baghouse filter and be
MDKM11AA U-234
U-235
U-238
No. of Results: 9
Sample Results Summary
TestAmerica
Ordered by Method, Batch No., Client Sample I D.
Result +-Uncertainty ( 2s) Qual Units
1.17E-02 +-1.9E-03 UCI/SA
4.21 E-04 +-1.2E-04 UCI/SA
1.12E-02 +-1.8E-03 UCI/SA
1.09E-02 +-1.BE-03 UCI/SA
4.48E-04 +-1.2E-04 UCI/SA
1.11E-02 +-1.8E-03 UCI/SA
4.22E-02 +-6.6E-03 UCI/SA
2.05E-03 +-3.9E-04 UCI/SA
4.31E-02 +-6.8E-03 UCI/SA
Date: 30-Apr-13
SDG No: 46619
Tracer
Yield MDL CRDL RER2
92% 5.B2E-05 9.00E-15
92% 3.22E-05 9.00E·15
92% 5.87E-05 9.00E-15
99% 4.45E-05 9.00E-15
99% 3.72E-05 9.00E-15
99% 5.16E-05 9.00E·15
92% 4.42E-05 9.DOE-15
92% 2.33E-05 9.00E-15
92% 3.28E-05 9.00E-15
TestAmerlca
rptSTLRchSaSum
mary2 V5.2.23
RKit2 -Replicpte Error Ratio~ (S.D)/(sqrt(sq(fPUs)+sq(TPUd))] ;~s defined by ICPT BOA.
• A2002
TestAmerica Page 6 of 15
Report No. : 55334
Batch
Work Order Parameter
FFSR
3104033 BLANK QC,
MOLDR1AA U-234
U-235
U-238
3104033 LCS,
MOLDR1AC U-234
U-238
No. of Results: 5
QC Results Summary
TestAmerica
Ordered by Method, Batch No, QC Type,.
Result +-Uncertainty ( 2s) Qual Units
2.37E-08 +-2.8E-08 u UCI/SA
-4.89E-10 +-1.2E-08 u UCI/SA
5.01E-08 +-3.9E-08 UCI/SA
9.06E-07 +-3.3E-07 UCI/SA
9.23E-07 +-3.3E-07 UCI/SA
TestAmerlca Bins -(Result/Expected)-I as deli ned by ANSI N13,30,
Date: 30-Apr-13
SDG No.: 46619
Tracer LCS
Yield Recovery Bias MDL
93% 4.66E-08
93% 2.46E-08
93% 4.19E-OB
93% 93% -0.1 2.90E-06
93% 91% -0.1 3.11E-08
rptSTLRchQcSum U Qunl-Analy.ud (or but not deteded nbove limiting crltorlq, Limit criteria I$ less thnn tbe Mdc/Mda!Mdl, Total Unccrt, CRDL, RDJ, or
mary V5.2.23 not ldcntllicd by gnmmn scon sortwnrc.
A2002
TestAmerica Page 7 of 15
~ CJ> ~ 3 ~ c;·
Q)
"U Q)
<C CD
co
~
~
CJ1
Lab Name: TestAmerica
Lot-Sample No.: J3D100435-2
FORM I
SAMPLE RESULTS
SDG: 46619
Report No. : 55334
Client Sample ID: X098 R1 NYC filters and beaker COCNo.:
Resnlt Count Total MDL, Rpt Unit, Yield Rst/MDL,
Parameter Qnal Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert
Batch: 31 04033 FFSR Work Order: MOKM21AA Report DB 10: 9MOKM21 0
U-234 1.17E-02 5.0E-D4 1.9E-03 5.82E-05 UCI/SA 92% (201.5)
2.17E-05 9.00E-15 (12.4)
U-235 4.21E-04 9.6E-05 1.2E-04 322E-05 UCI/SA 92% (13.1)
8.75E-06 9.00E-15 (7.3)
U-238 1.12E-02 4.9E-04 1.8E-03 5.87E-05 UCl/SA 92% (190.)
2.20E-05 9.00E-15 (12.4)
Ratio U-234/238 = 1.1
No. of Results: 3 Comments:
Date: 30-Apr-13
Collection Date: 4/3/2013 7:30:00 AM
Received Date: 4/10/2013 10:30:00 AM
Matrix: FILTER
Ordered by gJ~nt Semple 10, Batch No.
Analysis,
Prep Date
4/25/13 1 0:22 p
4/25/13 10:22 p
4/25/13 10:22 p
Total Sa
Size
1.0
Sample
to
Sample
1.0
Sample
Aliquot
Size
0.00119
Sample
0.00119
Sample
0.00119
Sample
Primary
Detector
ALP3
ALP3
ALP3
TestAmerica MDC[..,DA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTl.RchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Nida/Mdl, Total Uncert, CRDL, ROL or not identified by gamma scan software.
V5.2.23 A2002
a;!
CJ) ~ 3 ~ {1"
Q)
'U Q)
tC (1)
<0
8.
~
01
Lab Name: TestAmerica
Lot-Sample No.: J3D100435-3
FORM I
SAMPLE RESULTS
Client Sample 10: X099 R2 NYC filters and beaker
SDG: 46619
Report No. : 55334
COCNo.:
Parameter
Batch: 3104033
U-234
U-235
U-238
No. of Results: 3
Result
FFSR
1.09E.Q2
4.481UU
1.11E-02
Comments:
Count
Qual Error ( 2 s)
4.8E-04
9.8E-05
4.8E..Q4
Total .MDL, Rpt Unit, Yield Rst/MDL,
Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert
Work Order: MOKM31AA Report DB ID: 9MOKM310
1.8E-03 4.45E-05 UCIISA 99% (245.2)
1.51E-05 9.00E-15 (12.5)
1.2E-04 3. 72E-05 UCIISA 99% (12.)
1.15E-05 9.00E-15 (7.5)
1.8E-03 5.16E-05 UCIISA 99% (214.8)
1.87E..Q5 9.00E-15 (12.5)
Ratio U-2341238 = 1.0
....
Date: 30-Apr-13
Collection Date: 4/4/2013 7:30:00 AM
Received Date: 4/10/2013 10:30:00 AM
Matrix: FILTER
Qrdered by Client Sample 10, Batch No .
Analysis,
Prep Date
4125/13 10:22 p
4/25/13 10:22 p
4/25/13 10:22 p
Total Sa
Size
1.0
Sample
1.0
Sample
1.0
Sample
Aliquot
s~
0.00118
Sample
0.00118
Sample
0.00118
Sample
Primary
Detector
ALP4
ALP4
ALP4
TestAmerica MDCIMDA,Lc-Detection, ~lslon Level based on instrument background or blank, adjusted by the sample Efficiency, Yleld, and Volume.
rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria Is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not ldentlfted by gamma scan software.
V5.2.23 A2002
~----"'--------------------~------~---·-----··-···--·-·-·-"·. ---·----··
~ (/) J;
3 (!) ~-
"'
'U "' co (!)
~ 0 a
<.11
Lab Name: TestAmerica
Lot-Sample No.: J3D100435-1
FORM I
SAMPLE RESULTS
SDG: 46619
Report No. : 55334
Client Sample ID: X1 00 R1 Bag house filter and be COC No.:
Par:m~.eter
Batch: 3104033
U-234
U-235
U-238
No.ofResulbi: 3
Result
FFSR
4.22E-02
2.05E-D3
4.31E-02
Comments:
Count
Qual Error ( 2 s)
9.9E-04
2.2E-04
1.0E-03
Total MDL, Rpt Unit, Yield RstlMDL,
IJncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert
WorkOrder: MOKM11AA Report DB ID: 9MOKM11 0
6.6E-03 4.42E-05 UCI/SA 92% {955.)
1.43E-05 9.00E-15 (12.8)
3.9E-04 2.33E-05 UCIISA 92% (87.9)
3.81E-06 9.00E-15 (1G.6)
6.8E-03 328&05 UCl/SA 92% (1316.2)
8.53E-06 9.00E-15 · (12.8)
Ratto U-2341238 = 1.0
'""
Date: 30-Apr-13
Collection Date: 4/4/2013 9:00:00 AM
Received Date: 4/10/2013 10:30:00 AM
Matrix: FILTER
Ordered by Client Sample 10, Batch No.
Analysis,
Prep Date
4/25/13 10:21 p
4/25/13 1 0:21 p
4/25/13 10:21 p
Total Sa
Size
1.0
Sample
1.0
Sample
1.0
Sample
Aliquot
Size
0.00109
Sample
0.()()109
Sample
0.00109
Sample
Primary
Detector
ALP2
ALP2
ALP2
TestAmerica MDCIMDA,Lc-Detection, Decision Level based on Instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSample U Qual -Analyzed for but not det9Cted above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Unc:ert, CRDL, RDL or not identified by gamma scan software.
V5.2.23 A2002
;ol
~ ~ r;·
Ill
"U Ill <0 CD
~ .... a ....
01
Lab Name: TestAmerlca
Matrix: FILTER
Parameter Result Qual
Batch: 3104033 FFSR
U-234 2.37E-08 u
U-235 -4.89E-10 u
U-238 5.01E-08
No. of Results: 3 Comments:
Co ant
Enor(2 s)
2.8E-08
1.2E-08
3.7E-08
Total
Uncert( 2 s)
FORM II
BLANK RESULTS
MDL, RptUnit,
Lc CRDL Yield
Rst/MDL,
Rst/TotUcert
Woril: Order: MOLDR1AA Report DB 10: MOLDR1AB
2.8E-08 4.66E-08 UCI/SA 93% 0.51
1.50E-08 9.00E-15 (1.7)
1.2E-08 2.46E-08 UCI/SA 93% -0.02
4.02E-09 9.00E-15 -0.08
3.9E-08 4.19E-08 UC!/SA 93% (1 .2)
1.27E-08 9.00E-15 (2.5)
Ratio U-2341238 = 0.5
Date: 30-Apr-13
SDG: 46619
Report No. : 55334
.Analysis, Total Sa Aliquot Primary
Prep Date Size Size Detector
4/25/13 10:22 p 0.15 0.15 ALPS
Sample Sample
4/25/13 10:22 p 0.15 0.15 ALPS
Sample Sample
4/25113 10:22 p 0.15 0.15 ALPS
Sample Sample
TestAinerica MDC)MDA,Lc-Detection, Decision Level based on lns1rument background or blank, adjust~ by the sample Efficiancy, Yield, and Volume.
rptSTLRchBiank
V5.2.23 A2002
U Qual-Analyzed for llut not detected above limiting criteria. Limit criteria is less tlullllhe Mdc:/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by ga~a sean software..
·---·-----........ ~~----
rot "' s> 3 ~ c;·
Dl
"1J Dl cc CD
~
1\) a
~
01
Lab Name: TestAmerica
Matrix: FILTER
Parameter
Batch: 31 04033
U-234
U-238
No. of Results: 2
Jlesult Count
Qual Error ( 2 s)
FFSR
9.06E-07 1.5E-07
9.23E-07 1.5E-07
Comments:
Total
Uncert(2 s) MDL
FORM II
LCS RESULTS
SDG: 46619
Report No. : 55334
Expected Recovery, Report
Unit Yield &pected Uneert Bias
Analysis,
Prep Date
Wort< Order: MOLDR1AC Report DB ID: MOLDR1CS
3.3E-07 2.90E-08 UCI/SA 93% 9.73E-07 5.08E-09 93% 4/25/13 10:22 p
RecLimHs: 70 130 -0.1
3.3E-07 3.11 E-08 UCI/SA 93% 1.02E-06 5.32E-09 91% 4/25113 10:22 p
Rec Limits: 70 130 -0.1
TestAmerica
rptSn.Rchlcs
V5.2.23 A2002
Bias -(ResultJE:rpec:tedr 1 as defined by ANSI N13.30.
-----------------~-~:------------··'--'--~--
Date: 30-Apr-13
Aliquot
Size
0.12
Sample
0.12
Sample
Primary
Detector
ALP6
ALP6
m' "' )>
3 C1> ::0. (') Ol
"U Ol co C1> ...... w
Q, ......
01
Chain of
CUstody Record
Temperature an R9C81pt ---
Drinking Water? YasO NoD
Test America
THE LEADER IN ENVIRONMENTAL TESTING
-
Cllo!m l f'l"JI<C~ {]lQJ ' (;/)4iQof~.lftn:rOtl<..
Tetco I O~an Kitchen 1 l 4/5/2013 I I
~~ ~~ 1'fHS,.'>IlfJMH.d:>ir~~/!F&'(~ Ub~ ( ~.._ 391 East 620 ~outh __I ltso'l.~92~9_1Q6 . . . I ,.. of _::..__
a)r [ ·-• JISt.$ . sr.ClOI'lraa !.LsDContaa All8/ysis(Attacllli$U American Fork , LU.L [~03 Ro<U>o-.....,;--... 1 ~ moro SfJ8DeJtn'IS6d'd)
~~Md~(SQjj ~ytNII'Num._ J
Energy Fuels 2Q~~1St Quarter ' 1 . SpeclaJ ll"tSSIIJctJoo6
~~~No. Containers & • I o-COndiiJons of Receipt
Mtttrix PlB381'VIltivlfS :0: s a ;:l. I
Sampfe LD. No. mid D9s¢/JIIOII Dace Time ft 1i! "' ~ Q R -lli ~iii. ~ ~ ,i ~1 (C<mlalnets tot 88dJ =n~• may~ comblil•d orr one line) ~ .f 111 Ill ! !! ~ ~ -! ~:!!! rxioo R1 Baghouse1\l~erand beaker • 11 4/4/2013 l~i X X I I I \'f'YDX:. ("('\ \ I---. fX09BRi NYC filters and beaker 4/3no13_j L?..:~o f XJ x J U ~ , ofV"'\O~V\ J....
I X099 R2 NYC filters and beaker I _4/4/2013 I 7:30 j X x .. J 1 .. , ~Q~I(Y\ '::>
I
t
' ' --:::l-:::/0\~ ~oS -i
~~,~~~'~ I
\.":\~ S-<t.-,~ I
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1
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_.HilZMI/dliJrl/n:olion ~·"'~ ..;, (.Afetttrll!ybe~il~M<~relt!lntld 0 ~ 0 F1BtiJIMblo 0 Sl<tl hriiiW 0 /Won B · 0 l..'lllmllOm D Return To e5:m N Dbpo6al By Lab 0 AJdlivrJ For __ Uonl1l$ ~r diM 1 mcnthJ
Tum/llomd'Tt!»/!sq~JWJ r ~~~ISPtlliM
D 24 f/ciJJs rP 4B '*"1'1 0 7 o.a,..., D 14 oa,..., 0 21 OQyg 0 omor_as ~-method. _,I 11
r, 1-L rY-, l!f{~ ~~~~{o T-~~\~9..~ ~ .. ~ -tAU:.. 14-tb-1~ l~o~
? ' ~:r """-I 71:roa 2.~8y IJ . 10519 I TIITJ(f
tL RtJ/Jnq-By • • OrJQ> I Tsmtr: 3.-Br ll:l;oo» ,11m.
~~
When Complete Email to: Dean or Paul [e-mail]
lMTiflllfif"Km:\YRift!:ll<>!iRntldn:>CiiifilwlliiRi/J«r: CAIWIY·SIO'SIOiltilfli>Satrf*;~Ff~Qjjiy
.::. ...
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Test America
THE LEADER I" e.to!VIAONMENTAL TEEITlNG
Sample Check-in List
1()1>0 Cont.in~ GM S= Re.Wt (Aniock) ~lrnti•M~J
Sample GM Screen Result (Sample Receiving) -L\~lnhittl'\r]
Client: ::l:> f: W SDG #: L\ '-.Q\.D \ <=\ NA [ ] SAF #: NA ~
Date!Time Received:_
Lot Nll111ber: ···::::>SS::J\Ci)U..'7:>'~
Chain of Custody# ________ ·-----------------------------.,....
Shipping Container ID: ___________ N~ Air Bill Number: NA~
Samples received inside shipping container/cooler/box Yes~ ] Continue with 1 through 4. Initial appropriate response.
No [ ] Go to 5, add comment to #16.
1. Custody Seals on shipping container intact? Yes [ No [ No Custody Seal ~ ]
Yes [ No [ No Custody Seal\) ]
_____ °C NA~ ]
NA [ Wet [ ] Dry~
2. Custody Seals dated and signed?
3. Cooler temperature:
4. Vermiculite/packing materials is
Item 5 through 16 for samples, Initial appropriate response.
5. Chain of Custody record present? Y<l~] No[
6. Number of samples received (Each sample may contain multiple bottles):__, ______________ _
8.
9.
10.
11.
Sample holding times exceeded?
Samples have:
___ tape
___ custody seals
'x::
A (FLT, Wipe, Solid, Soil)
S (Air, Niosh 7400)
NA[ Yes[
~hazard labels
~appropriate sample labels
__ I(Water)
__ T (Biological, Ni-63)
No[~]
~,;npi=~ in good condition -~are leaking -1(--are broken __ have air bubbles (Only for samples requiring no head space) ====Oili~------------------------------------------------------------------------
12. Sample pl-1 appropriate for analysis requested Yes [ ] No [ ] NA fit ]
(If acidification is necessary, then document sample ID, initial pH, amount ofHN03 added ~pH after addition on table overleaf)
RPL ID #of preservative used :.-"-"~1-.l~------------------------------
13. Were any anomalies identified in sample receipt? Yes [ ] No~ 1
14. Description of anomalies (include sample numbers): NAY-----------------------
LS-023, Rev. 15, 07/11 See over for additional information.
TestAmerica Page 14 of 15
Test America
'rHE LE ... OER IN E;NVIRONMENTAL.. TESllMG
15. Sample Location, Sample Collector Listed on COC7 *
"'For documentation only. No corrective action needed.
Sample Custodian: . ~ ~
[ ] Cli~UCoud" den;~-oho<k.
Yes [ ] No~ ]
] Client/Courier unpack cooler.
Date: L.\-\0--\ ~
Client Informed on. ________ by _________ Person contacted. ________ _
1}(1 No action necessary; process as is
ProjectMan~~gar ~ ~ CJDJ~ Date l/-/ Z..::t\3
SAMPLEID Initial pH Acid Amt Final pH SAMPLEID Initial pH AcidAmt Final_llH
'\ 1\
\ \
\ '\
\ '\
\ ~
\ ~
\ '\
\ A \
/ ~~ \ A
\..... ~ ~71
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I\' ;:. ~h
\ 1 ~')
\ 1 \
\ \
\ i\
\ \ \
\
1\ '·
J
\
\
LS-023, Rev. 15, 07111 See over for additional information.
TestAmerica Page 15 of 15
APPENDIXD
South Yell ow Cake Scrubber
Figure 1. Facility Schematic Representation
Yell ow Cake Dryer Baghouse
Figure 2. Facility Schematic Representation
Production and Control Equipment Data
South Yellow Cake (Scrubber Flow Rates)
Yellow Cake Dryer Baghouse (Delta P readings on Field Data Sheets)
D
Fadlity: Energy Fuels Resources
t
a
t
y
Stackldentification: South yellow Cake Scrubber
l+--0~1
~
a: Distance upstream from next disturbance, feet -----
~: Distance downstream from last disturbance, feet
0: Stack Inside Diameter, inches --
Estimated Moisture, percent
Estimated Temperature, '1'
Estimated Velocity, fpm
Control Unit
Type:
Scrubber
Number of Ports
-----
Figure 1. Facility Schematic Representation
Process
Type:
Yell ow Cake Processing
F•dlity, Energy Fuels Resources
t
a
~
y
stackidentification: Yellow Cake Dryer Baghouse
l+--0-+l
~
a: Distance upstream from next disturbance, inches
~: Distance downstream from last disturbance, inches
y: Distance of Sample Level to Ground, feet
0: Stack Inside Diameter, inches
Estimated Moisture, percent
Estimated Temperature, °F
Estimated Velocity, fpm ___
Control Unit
Type:
Baghouse
Number of Ports 2
57"
454"
65'
16"
0-2%
125
1,400
Figure 2. Facility Schematic Representation
Process
Type:
Yellow Cake Processing
Energy Fuels Resources, Blanding, UT Process Data
Source: South Yellow Cake Date: '( 7) j, :3
Scrubber Flow GPM
Time #1 #2 6P
T .'3D ~cJ. 4 1()·1-
f;ov :,a·! l c) ·1-
~:Jo ") t.o I u ,-:f
q:,..-oo )\. '\ t C>·~
-
;;:; :1 0 ) \ ·\ l u . -:t-
t () : oo "L __ , .. D I . I --j
~~ : \..I I I
/D.' 3D 7_' :) ; :_j . : -z ,: -'
I~.' oo . ~ ··. . ') . -. .-.1
\. .... ) . >,:~ .. 1 I '1 , ~_) ~·f
';> ... ,-•
t ~z· ~ : .. ~ () ~·;· .. ,.'I I -· I
-~ l ><{
. ' ' fO ·+ I 4 (I ~ ,_} "3 f, ~ . .,. ' ~ ~1.-""L l () ·1-•. -..
.. ''Z. . l-:J (D ~-+ '· -·· -,
'·
1 (.r ()0 ~7· 0 \ D ·1-
t '-1 ~ ~() ~ -s.-:s {0'--:;f
)]• 7
\~: 00 ~ 7 ·) ( () ·1 . )D J '$• "L (5" . ~ f. ·r
I oO t l9 • -; ? . \ l D·1
Energy Fuels Resources, Blanding, UT Process Data
Source: South Yellow Cake Date: 4 ~I ()
Scrubber Flow GPM
Time #1 #2 l!.P
1 .') () 5?-·'i t6 .-::)_
cr:vo ~(. ~ 3't (4 -::]
~ .· 3 c) )?.. . C> I 0 ·-;}
I
~: Oo ~~-~ ;y4 {D· ~
c, . )6 ~ \· ~ to·--;f
!0 ·. Do -,-z..·7 lv·1
[{J: ~ 1~· \ ro·t-
I( ; oo 7t·-()-( b·r
vi : 10 ) 1-. 1 ( 0·~
,z. ; oo ~l-LI (0·1----
! t : ~0 ~"'Z·) 1 () . 1-
(> ·. oo ) z_, 5 ['\.). i
3 • ) D I . 7'2·0 ro·Sf-
lc.f:'"'o ~1---D /b ·1
ty :-so ~z ·7 \0.~
•. 0~ l S' . "}1· ...( 1 0. 1
rs-·. 3o '2 ~. ~ (n.q
'
APPENDIX£
Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature
sensors were carried out in accordance with the procedures outlined in the Quality Assurance
Handbook. The appropriate calibration data are presented in the following pages. The nozzle
calibrations are recorded on the first page of the field data sheets.
Figure 3 Schematic of Method 51114 Sampling Train
Meter Box Calibration Data and Calculations Forms
Post-test Dry Gas Meter Calibration Data Forms
Type S Pitot Tube Inspection Data
Sample Box Temperature Sensor Calibration
E
~Senso'
~Probe
TypeS Pilot
Tube
Te~~~~~~re
Gooseneck
Nozzle j -1--WTra::ed
""
Ga;a1lra1 / A'd:e. -----,.
/
TypeS Pitot
Tube ~
Temperature
Sensor
Glass Filter
Holder
Heated Area
lllllingerTrain Q:ltlonal, M:IY Be Replaced
By An E~ulvalent Condenser
J
Temperature
Sensor
,---------------
lmpingers
Stack
Wall Manometer Water Empty Silica
Gel
Orifice
Dry Gas
Meter
Air-Tight
Pump
Figure 3 Schematic ofMethod 5/114 Sampling Train
Vacuum
Line
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Select three critical orffices to calibrate the dry gas meter which bracket the expected operating range. E !!iffiM!QfiM!&M!Hllii¥ -C" -"" ~ i) .... -..,. _ _,, V'~".y" ··~ .
2) Record barometric pressure before and after calibration procedure.
3) Run at tested vacuum (from Orifice Calibration Report). for a period of time
necessary to achieve a minimum total volume of 5 cubic feet.
4) Record data and information in the GR£ErJ cells. YELLOW cells are calculated,
METER SERIAL/I:' -----I
CRITICAL ORIFICE SET SERIAL IJ: 14535 EQUIPMENT tD #:
K' TESTED
r-----,-----1 FACTOR [VACUUM
RUNII I (AVG) (in Hg)
~]: 0.8137 12
0.8137 12
0.6137 12
128.204
133.568
139.020
G: 0.5317 13
0.5317 13
0.5317 . 13
95.7570
100.951
106.479
G: 0.3307 20
0.3307 20
0.3307 20
111.900
117.108
122.339
USING THE CRITlCAL ORIFICES AS CAUBRATION STANDARDS:
FINAL
133.588
139.020
144.448 I
100.951
106.479
111.698
117.108
122.339
127.559
5.384
5.432
5.428
5.194
5.528
5.219
5.208
5.231
5.220
70 78
70 IU
70 85
I 70 69
I 70 70
I 70 70
70 74
70 75
70 75
83
85
86
70
10
'---73
75
76
77
76
84
93
68
71
.72
75
76
77
84
93
94
71
7~
75
76
77
78
DGM
AVG
79.75
86.25
89.50
69.75
70.75
72.50
75.00
76.00
76.75
IJ
FlNAL
[ 25.45 J
ELAPSED
TIME(MtN)
a
AVG(P,M)
25.45
§§60
2.60
2.60
7.50
s.oo
7.50 1.11
12.00
12.00
12.00
§ 40
0
4.5144
4.5004
~
4.4194
~
~
YZZ§
~
4.3736
2013 Pre~Calibration
IF Y VARIATION EXCEEDS 2.00%,
ORIFICE SHOULD BE RECALIBRATED
l
4.4990 .Mll
4.4990 1.000
4.4990 ~
AVG= 1Jm1 0.01
4.4097 ~
!.Zill ~
!..4lli. 2.m.
AVG= ~ ::2..11
4.3883 1.W
Ylli 1.&Q!l
~ 1.W.
AVG~ ~ Q..11
1,lli.
1,ill
1.488
!.ill
~
.!,lli
1.ill
1.ill
1.410
The following equations are used to calculate lhe standard volumes of air passed through the DGM, V rn (sld), and the critical orif;ce,
V ~ (std). and the OGM calibration factor, Y. These equaUons are automatically calculated in the spreadsheet above. AVERAGE CRY GAS METER CALIBRATION FACTOR, y = ( 1.001 I
(1)
(2)
(3)
Vm'.·""' = K, • vm.'Pbor"-(tlH /13.6) rm
?bar* e
Vcr,,,l) = K'• .JTamb
= Net volume of gas sample passed through DGM, corrected to standard conditions
K, -17.64 'Riin. Hg (English). 0.3858 'Kimm Hg (Metric)
T m;:; Absolut-e DGM avg temperature {0R -English, °K-Metric)
=Volume of gas sample passed throllgh the critical orifice, corrected to standard conditions
r.~ = Absolute ambient temperature (0R -English, °K-Metnc)
K' :; Average K' factor from Critical Orifice Calibration
Vc1i.ud' Y= --= DGM calibration factor
Vml,_~'·"
AVERAGE &HI!:[ I
2 t:.HA = ( 0.75 9 ) t:.H (Vm(std))
v.,(std) vm
Temperature Sensors
Reference In Out
"F OF "F
32 33 32
72 73 73
203 202 202
Pre 2013 5 console
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES ~-t~'--'f: g !#W !Ai&@#J¥iiLF-_ .. .:a....-=.-.=·
t .
1) Select three critical orifices to calibrate lhe dry gas meter which bracket the expected operating range.
2) Record barometric pressure before and afler calibration procedure.
3) Run attested vacuum (from Orifice Calibration Report), for a period of time
necessary to achieve a minimum total volume of 5 cubic feet.
4) Record data and information in the GHEEN cells, YELLOW cens are calculated.
METERSERIAL J:I ·······~-~
CRITICAL ORIFICE SET SERIAL 1: 14535 EQUIPMENT 10 •:
K' TESTED
.-------~---1~FACTORIVACUUM
J J RUN f (AVG) (In Hg)
INITIAL
DGM
AVG
FINAL ry:;J
ELAPSED
TIME(MIN)
e
ENVIRONMENTAL SUPPLY COMPANY
AVG(P..,)
25.20
2013 Pre-Calibration Console 9
IF YVARIATlON EXCEEDS 2.00%,
ORIFICE SHOULD BE RECALIBRATED
1
0
G
G
~
0.8U7
0.8137
0.8137
1~
12
12
4DS.S71 4tl.164
411.964 417.814
417.814 4U.674
6.385
5.850
5.860
TD
7D
70
76 78
78 80
BO 81
73 74
74 74
74 74
75.25
76.5
77.25
§§.00
l .OD
l.OO
5.3623
4.8924
4.B9lt
.Yill.
4.9002
!.!W.
l!.ll!
~
Ml!!
!,ill.
!.ill.
Lill
l
1
~
0.5317
0.1317
0.1317
D.J307
O •. J307
0.3307
12 381.103
12 ll3.l"!'1
12• 318.&32
u 424.550
11 UIUB1
13 4U.011
USING TfiE CRITICAL ORIFICES AS CAUBRATION STANDAADS:
383.271
UU31
403.684
421.881
43S.011
440.174
5.158
U61
5.152
5.331
5.130
5.163
70
70
70
75
75
75
n 72
12 75
71 T7
77 77
77 78
7! 78
41.
·.72
n
7'
74
74
72
12
72
74
74
74
64.60
72.75
74.00
75,50
75.75
78.00
7.60
7.60
7.50
12.00
12.60
12.00 § 44
44
4.3980.
Mill
4.3063
~
4,2644
~
AVG2
4,3663
4.lliJ.
4.3663
AVG•
w.n
um
!.ill!
AVG•
Ml!! :Y!
!b!ll
l!.lli
1M!
MH. ~
Lill.
!.ill
.1.2M
.1.ill. llli.
1..lli.
1.ill.
.!.,ill
!.ill.
1..rn
!.ill.
The following equations are used lo calculate toe standard volumes o! air pa$Sed through the DGM, V~ (sld), and the critical orifice,
V~ (sld), and the DGM calibration factor, Y. These equations are automatically calculated in the spraadsheelabove. AVERAGE DRY GAS METER CAUBRATION FACTOR, y =I 1.004 I
(1)
(2)
(3)
Vmr.,,,, = K, • Vm • Pbnr• CLIH l l:l tl) rm
/'/Jar. e Vt.·r< .. ,.,1 = K'• ~h--
= Net volume of gas sample passed through DGM, corrected to standard conditions
K, = 17.64 'R~n. Hg (English). 0.3858 'Kimm Hg (Metric)
T,., = Absolute DGM avg. temperature ("R -English. =K-Merrie)
:o:: Volume of gas sample passed fhiOUgh !he critical orifice, corrected to standard conditions
T.nil = Absolute arnbier.t temperature ("R • Er.glish, °K-Me~ric)
K' = Averag-e K' factor from Critical Orifice Calibration Vc'\,1J1 Y= -Vm1,.,,;1
= DGM calibration factor
AVERAGE ~H. =J 1.679 I
t.HI!!l = ( .2,lli )! 6fi (Vm(std))
V"(std) Vm
Temperature Senson;
Reference In Out
aF aF °F
32
72
7.01
33
73
202
33
73
203
Console 9 Pre-test 2013
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.
2) Record barometric pressure before and after calibration procedure.
3) Run at tested vacuum (from Orifice Calibration Report), for a period of time
necessary to achieve a minimum total volume of 5 cubic feet.
4) Record data and information in the GREEN cells, YELLOW cens are calculated.
K' TESTED
.--------.------1 FACTOR I VACUUM
] ] RUN # I (AVG) (In Hg)
METER SERIAL I:~
CRITICAL ORIFICE SET SERIAL i:~ EQUIPMENT 1D II:
o:rn~ .0
.0
.0 1-f-f T II
G: 0.53t7 12
0.5317 12
0.5317 -12
861.050 866.129
8&8.129 871.60
871.60 877.442
o:rn~
USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
5.079
5.471
5.842
.0
.0
.0
83 56 eo 60 62
u 60 62 62 66
63 62 66 64 65
D-1111
DGM
AVG
0.00
0.00
0.00
59.50
62.50
64.25
0.00
0.00
0.00
FINAL
I 24.85 I
ELAPSED
TIME(MIN)
9
AVG(P.,,)
24.85
§§
§,..--,.
DO
50
1.10
§§
4.3022
4.§076
~
Energy Fuels
IF Y VARIATION EXCEEDS 2.00%,
ORIFICE SHOULD BE RECALIBRATED
AVG=
4.3344
4.6234
4.9124
AVG=
AVG=
(3)
y
1.007
1.003
.l!!!!l
1.004
1
I VARIA~ON (%)
!!.!!!!
1.569
1.560
1.555
The following equations are used to calculate the standard volumes of air passed through the DGM, V., (std), and the critical orifice,
V., (std), and the DGM calibration factor. Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y" Q00~
(1)
(2)
(3)
Vm,,,.> = K, • Vm• Pbar+(M !13.6)
Tm
Pbar *0
VcrC••'> = K'• .JTamb
= Net volume of gas sample passed through DGM, corrected to standard conditions
K, = 17 64 "Riin. Hg (Englis~). 0.3858 "Kimm Hg (Metric)
T., = Absolute DGM avg. temperature ('R-English, 'K-Metric)
= Volume of gas sample passed through the critical orifice, corrected to standard conditions
T,.,.., =Absolute ambient lemperalure ('R-English, 'K-Metric)
Vcr<lldJ Y= --
Vm(utJJ
K' = Average K' factor from Critical Orifice Calibration
= DGM calibration factor
AVERAGE AHg =[ 1.561 I
2
h.Hg = ( 0.76 9 ) &H (Vm(std))
V0,(std) Vm
Temperature Sensors
Reference In Out
"F
32
72
203
"F
33
73
202
"F
32
73
202
post 2013
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.
2) Record barometric pressure before and after calibration procedure. ENVIRONMENTAL SUPPLY COMPANY
3) Run at tested vacuum (from Orifice Calibration Report), for a period of time
necessary to achieve a minimum total volume of 5 cubic feet.
4) Record data and information in the GREEN cells, YELLOW cells are calculated.
METER SERIAL ""I ·~·· ""£~~ l
CRITICAL ORIFICE SET SERIAL 1l: 1453S EQUIPMENT 10 II:
K' TESTED
FACTOR I VACUUM I l RUN# I (AVG) (in Hg)
om~ .0 III!-§ .0
.0
G: 0.6808 12
0.5808 12
0.6808 12
545.903 551.219
551.219 55$.1165
556.965 562.719
om~
USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
5.318
5.746
5.754
.0
.o
.0
62 65 66 60 65
62 66 6B 65 68
62 68 72 66 67
r -1-1 r 1-1
DGM
AVG
0
64.00
66.25
68.25
0.00
0.00
0.00
FINAL
[ 24:;]
ELAPSED
TIME {Iollfol!
9
AVG(P .. ,)
24.85
§§
§ 0
50
§§
~
4,8174
~
Energy Fuels
IF Y VARIATION EXCEEDS 2.00%,
ORIFICE SHOULD BE RECALIBRATED
l
AVG=
4.4442 ~
4.8145 ~
4.8145 .1Jm
AVG= ~ 0.00
AVG=
The following equations are used lo calculate the standard volumes of air passed Ill rough lhe DGM, V. (std), and the critical orifice,
V a (std), and the DGM calibratiOn factor, Y. These equations are automatically calculated in the spreadsheetabcve. AVERAGE DRY GAs METER CALIBRATION FACTOR, v =I o:9s8]
(1)
(2)
(3)
Vm,,,1 = K, • Vm • Pbor + (M//13.6)
Tm
Pbar • 0
Vcr''"'' = K'• .JTamb
= Net volume of gas sample passed through DGM, corrected to standard conditions
K, = 17 64 "Riin. Hg (English), 0,3858 'Kimm Hg (Metric)
T m = Absolule DGM avg, temperature ("R-English, 'K ·Metric)·
= Volume of gas sample passed through the critical orifice, corrected to standard conditions
T...., = Absolute ambient lemperature ('R -English, 'K-Metric)
K' = Average K: factor lrom Critical Orifice Calibration
Vc'(,rd) Y = --= DGM calibration factor
Vm{.r/J)
AVERAGE !l.H@I =I 1.719 I
2 AH~ = ( 0.75 0 ) AH (Vm(std))
Vcr(std) Vm
Temperature Sensors
Reference In Out
OF
32
72
201
"F
33
73
202
OF
33
73
203
1.,ill
!.ill
.!.,ill
Console 9 Post-test 2013
/) (\i
.----./AJ ~ \ ~ .. .-13\
'-J p.:
f ,,. .,... ... •.. .( )'
T~ pL S Pilot Tube lnspl!..::lil~n Da1:.1
hhr.:~•~n -tC-M t:-tJ ct."-\ o.-r ~
0:= . ~~~'"
P,= ,t.f.lj"
'"'-"f',_= -·=--'t~1_._____,.{g'-_ ..
~: < 5'
\\' s 1) 031~5 in
\\' > ~ ir:~h:!5
l > 3..! (;:.:}]
(.:_:;;; ____ _
~ C<; = _ ___,..___ __
[l; = ---=~;.__-
~:= __ t. __ _
Z= • Do'
\'.'= . 00 t 1::
\\ = (p 'tz_ ir.
Z= !::
B~--.. .r-____ ,.~: ,-c··.:; y ,.. __ J_~ ..... ~~-'c
Typ~ S l'iwl Tube lnsr:.:clion D~t:!
f.' hhr.:c,,~ ----t<". M £. N 41\..~~----
t ~----..--r----:;:::,/ "f FA
~ • ::::--..,. 1 • < -·-...______,!: ___ .. _,._
[):~_. > 1~ _1'\ I; p, ~ PR •)
-j"-"="--'------
1:> ;~ • D, ~ Ll. ~; l :·.' • D, ·.' -~..::.~~-----
"' ~ "'2--
«;~ 0
r>, < s·' r:.: -
r.: < 5) P: = .•
z~ btl I;:
~-··-··-~-· \\" .-J'0=--0 ..... -.~-·-· \\' 5 ·) o:.t.:!s ir: \\'= .o l5" I::
\\'= \ Jr,
Z= If.
1 = ..., 'A. ~·: ~-~~-
~l)IL \\'.'.TfR ll 1 ~ ~ o Ul I()
SILICO:\E 0!~ ~
ij
TETCO
Sampk l3ox Temperature Sensor Calibration
Date' 12/19/12 Calibrator: Mike McNamara Reference: Omesa CL3512A
Thermocouple Temperature Temperature Temp. ()iff.
lJnit ID Location Source Reference Sensor or Result
{Mcdlmi\l C'Fl ('F) ('F), P/F
Oven Water 33 34 I
Water 204 204 0
II A Water 33 I 34 I I
Probe Out Water 204 204 ()
lmpinger Out Water I 33
I!
34 ---1 l
Water 204 204 0
Oven I
Water ~-33 35 2
Water 204 204 0
B Probe Out I Water
II
33 35 2
Water 204 204 0
lmpingcr Out Water
-I
33
II
34
I
I
Water 204 204 0
Oven I
Water
II
33
!I
34 I I
Water 204 204 0
c Probe Out Water 33 34 I
Water 204 204 0
lmpinger Out Water 33 34 I
Water 204 204 0
Oven Water
I
33
I
33 0
Water 204 204 0
D Probe Out Water 33 33 0
Water 204 204 0
lmpinger Out Water 33 -I 34 I I
Wnlcr 204 203 -l
Oven Water 33
I
34 I I
Water 204 204 ()
E Probe Out Water 33 34 I
Water 204 204 0
Impinger Out Water 33 34 I
Water 204 202 -2
Oven I
Water
II
33
II
34 1
Water 204 204 0
F Probe Out l Water I 33 34 I
Water 20 204 0
Impinger Out \Vater 33 35 2
Water 204 202 -2
~~~~ lmpinger Out 0 I Water l 33 I 34 I l ~~ :~: .' ~] Water 204 202 -2
~-;rt~ ~% ~ « lmpingcr Out H I
Water
II
33 ll 35 I 2
Water 204 202 -2
~"<.·~ . ..,r.~T-;· lmpingcr Out I Water 33 34 J
~ ~~f~~ Water 204 204 0
~t!~ 1)~~ <
I Water 33 34 I ...... lmpinger Out J Water 204 203 -·I
p.•~ lmpinger Out K Water I 33
II
34
I
I
~ "'"· . ~ Watet 204 204 0 ::;;. . -y;:_}':-'1~~·· i '~it..'> ~-:.;i>.:.:.~l ~
APPENDIXF
The testing followed the same procedures as outlined in previous protocols and tests at this
facility.
Prepared for:
Energy Fuels Resources
6425 S Hwy 91
Blanding, Utah 84511
Date of Report:
July 29, 2013
SECOND QUARTER
RADIONUCLIDE EMISSIONS TEST
CONDUCTED AT
ENERGY FUELS RESOURCES
SOUTH YELLOW CAKE SCRUBBER
YELLOW CAKE DRYER BAG HOUSE
GRIZZLY BAGHOUSE
BLANDING, UTAH
April3-4, 2012
June 5-6, 2013
by:
TETCO
391 East 620 South
American Fork, UT 84003
Phone [phone]
Fax [phone] fax
CERTIFICATION OF REPORT INTEGRITY
Technical Emissions Testing Company (TETCO) certifies that this report represents the truth as
well as can be derived by the methods employed. Every effort was made to obtain accurate and
representative data and to comply with procedures set forth in the Federal Register.
Dean Kitchen
Rcviewer:. ____ _.A~!Pt:c--....:::· -=-,~,&"-~--':JL...o=:=----
Date:. ______ --'7'---->',h"'""· _._j'_-___;_.,1,""'7_-----"-__ _
I< iewer: f,J tiL -Mike McNamara
Date: -1{ 'l <t {c~
ii
TABLE OF CONTENTS
Introduction
Test Purpose ............................................................ 1
Test Location and Type of Process ............................. _ ............. 1
Test Dates ............................................................. 1
Pollutants Tested and Methods Applied ...................................... 1
Test Participants ......................................................... 2
Deviations From EPA Methods ............................................. 2
Quality Assurance ....................................................... 2
Summary of Results
Emission Results ........................................................ 3
Process Data ............................................................ 3
Description of Collected Samples ........................................... 3
Discussion of Errors or Irregularities ......................................... 4
Percent Isokinetics ....................................................... 4
Source Operation
Process Control Devices Operation .......................................... 5
Process Representativeness ................................................ 5
Sampling and Analysis Procedures
Sampling Port Location ................................................... 6
Sampling Point Location .................................................. 6
Sampling Train Description ................................................ 7
Sampling and Analytical Procedures .......................................... 7
Quality Assurance ....................................................... 7
Appendices
A: Complete Results and Sample Calculations
B: Raw Field Data
C: Laboratory Data and Chain of Custody
D: Raw Production Data
E: Calibration Procedures and Results
F: Related Correspondence
iii
LIST OF TABLES
Table
I Measured Radionuclide Emissions .......................................... 3
II Percent Isokinetics ....................................................... 4
III Sampling Point Location .................................................. 6
IV Complete Results, South Yellow Cake Scrubber ...................... Appendix A
V Complete Results, Yell ow Cake Dryer Baghouse ...................... Appendix A
VI Complete Results, Grizzly Baghouse ............................... Appendix A
LIST OF FIGURES
.,.igure
I racility cbematic Repre entation ouU1 Yello Cak Scrubber .......... Appendix D
2 Fa ility Sehematic Repres.entation Yellow ake Dry r Baghouse ......... Appendix D
3 Facility chetnatic Repre emation GrizzJy Bai:'>hous ................... Appendix D
4 chematic fMethod 5/114 . ampling Train .......................... Appendix E
iv
INTRODUCTION
Test Purpose
This test project was conducted to determine the total radionuclide emissions from the South
Yellow Cake Scrubber, Yellow Cake Dryer Baghouse, and Grizzly Baghouse exhausts in terms
of Curies per dry standard cubic foot (Ci/dscf).
These tests were for U-N at and Th-230 on the Grizzly Baghouse and U-Nat, Th-230, Ra-226,
and Pb-210 on the South Yellow Cake Scrubber and Yellow Cake Dryer Baghouse.
Test Location and Type of Process
Energy Fuels Resources is located about 5 mile south of Blanding tah. ranium re i
processed into yellow cake, which is shipped to other fa.cili ies for additional proce sing. There
are two yellow cake dryers with individual scrubber . Botb dryer enclo ure di charg int the
Dryer Baghouse. The Packaging enclosure also discharges into the Dryer· Baghou e. The South
Yell ow Cake (NYC) dryer was the only operating dryer. at the time of the test. The North
Yell ow Cake Dryer was not operating at the time of the test. The Grizzly Baghouse serve as the
main dust control device for the raw ore unloading and conveying to the processing building.
Stack schematics are shown as Figures 1 though 3 in Appendix D.
Test Dates
The first test run on the SYC Scrubber was completed April 3, 2013. The second test run was
completed April4, 2013.
One test run was completed on the Yellow Cake Dryer Baghouse April4, 2013.
One run was completed on the Grizzly Baghouse June 5-6, 2013.
Pollutants Tested and Methods Applied
The tests were a determination of radionuclide emissions in accordance with EPA Method 5/114.
Test run filters and front wash residues were sent to Test America located in Richland,
Washington for radionuclide analysis.
Test Participants
Test Facility
State Agency
TETCO
Garren Palmer
None
Doug Olsen
Jeff Graton
Deviations From EPA Methods
None
Quality Assurance
Mike McNamara
Testing procedures and sample recovery techniques were according to those outlined in the
Federal Register and the Quality Assurance Handbook for Air Pollution Measurement Systems.
2
SUMMARY OF RESULTS
Emission Results
Table I presents the findings of the test in Curies per dry standard cubic foot. Tables IV-VII in
Appendix A have more detailed information.
Table l. Measured Radionuclide Emissions
South Yell ow Cake Yell ow Cake Dryer Grizzly Baghouse
Run# Scrubber Baghouse *
pCi/dscf pCilhr pCi/dscf pCi/hr pCi/dscf pCi/hr
I 83.2 9.378E+06 1112.3 2.261E+08 0.482 4.028E+04
2 80.9 9.221E+06 I
AVE 82.0 9.299E+06 1112.3 2.261E+08 0.482 4.028E+04
* Dryer Baghouse results are only for U-Nat
Process Data
The process was operated according to standard procedures. All pertinent process data was
available for recording by agency personnel. Scrubber water flow, pressure drop readings (!1p)
were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (!1p)
were recorded and are found on the test run sheets. Production data is retrained bEnergy Fuels
Resources.
Description of Collected Samples
The test filters for the South Yell ow Cake Scrubber were heavily covered with an off-white
colored particulate. The front washes were clear in appearance.
The test filters for the Yell ow Cake Dryer Baghouse were lightly colored with a tan colored
particulate. The front wash was clear in appearance.
The test filters for the Grizzly Baghouse were had no visible particulate. The front wash was
clear in appearance.
3
Discussion of Errors or Irre2ularities
The sample analyses for the SYC and Dryer Baghouse were initially completed for U-Nat and not
the other radionuclides. After conferring with Energy Fuels Resources representatives and
approximately three weeks after the initial sample analyses, Test American was contacted to see
if the samples could be analyzed for Th-230, Pb-210 and Ra-226. Test American indicated that
there was sufficient sample to run the additional analyses. A separate laboratory report from Test
America was completed for the additional analyses.
Because of a communication error in requesting the additional analyses, the Dryer Baghouse
samples were not analyzed for Th-230, Pb-21 0, and Ra-226. The Dryer Baghouse results are for
U-Nat only. However, it should be noted that during the 4th quarter 2012 test project that the U-
Nat results for the Dryer Baghouse were more than 3 orders of magnitude greater than the
combined Th-230, Pb-21 0, and Ra-226 sample results.
Percent Isokinetic Sampling
Each of the tests were isokinetic within the ±10% of 100% criterion specified in the Federal
Register. They also meet the Utah State Department of Environmental Quality, Division of Air
Quality specification of isokinetic sampling point by point. Isokinetic values for each test run are
presented in Table II.
South Yell ow Yellow Cake Grizzly
Run# Cake Scrubber Dryer Baghouse Baghous
1 101
I
101 94
2 99
4
SOURCE OPERATION
Process Control Devices Operation
All process control devices were operated normally. Recorded scrubber water flow, pressure and
baghouse ~p readings were recorded and are found on the test run sheets or in Appendix D.
Process Representativeness
The facility was operated normally. Production data was retained by Energy Fuels Resources.
5
SAMPLING AND ANALYSIS PROCEDURES
Sampling Port Location
The inside diameter of the South Yellow Cake Scrubber stack is 12.75 inches. The two, four-inch
diameter sample port are located 28.24 diameters (30 feet) downstream from the last disturbance
and 6.59 diameters (7 feet) upstream from the next disturbance. Figure I in Appendix D is a
schematic of the stack.
The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch
diameter sample ports are located 28.38 diameters (454 inches) downstream from the last
disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port
locations are depicted in Figure 2 in Appendix D.
The inside diameter of the Grizzly Baghouse stack is 18.75 inches. There are two, three-inch
diameter sample ports located 2.56 diameters (48 inches) downstream from the last disturbance
and 1.31 diameters (24.5 inches) upstream from the next disturbance. The sample port locations
are depicted in Figure 3 in Appendix D.
Samplin2 Point Location
Table III shows the distance of each sampling point from the inside wall according to EPA
Method 1. Each point is marked and identified with a wrapping of glass tape and numbered.
These points are determined by measuring the distance from the inside wall.
Sample Point
2
3
4
5
6
7
8
9
10
11
12
0.85 0.70 0.50
3.19 2.34 1.26
9.56 4.74 2.21
11.90 11.26 3.32
13.66 4.69
15.30 6.68
12.08
14.06
15.43
16.54
17.48
1825
6
Sampling Train Description
To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-51114
were followed.
All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent
interference of the sampled gas and particulate.
The stack analyzers used to conduct Methods 1-5/114 are constructed to meet the specifications
outlined in the CFR. The temperature sensors are K-type thermocouples. Heater, vacuum and
pitot line connections have been designed to be interchangeable with all units used by the tester.
A 316 stainless steel probe liner was used for the tests. Figure 4 in Appendix E is a sketch of the
Methods 5/114 sampling train.
Sample boxes were prepared for testing by following the prescribed procedures outlined in
Methods 5/114.
Sampling and Analytical Procedures
All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A,
Methods 5/114.
Quality Assurance
All equipment set-up, sampling procedures, sample recovery and equipment calibrations were
carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance
Handbook for Air Pollution Measurement Systems.
7
APPENDIX
A: Complete Results and Sample Calculations
B: Raw Field Data
C: Laboratory Data and Chain of Custody
D: Raw Production Data
E: Calibration Procedures and Results
F: Related Correspondence
8
APPENDIX A
Table IV Complete Results, South Yellow Cake Scrubber
Table V Complete Results, Yellow Cake Dryer Baghouse
Table VI Complete Results, Grizzly Baghouse
Nomenclature
Sample Equations
A
TABLE IV SYC Scrubber
COMPLETE RESULTS
Energy Fuels CORPORATION, BLANDING, UTAH
SOUTH YELLOWCAKE SCRUBBER EXHAUST
Symbol DescriEtion Dimensions Run #1 Run#2
Date 4/3/13 4/4113
Filter# X098 X099
Begin Time Test Began 7:47 7:34
End Time Test Ended 15:51 15:37
Pbm Meter Barometric Pressure ln. Hg. Abs 24.50 24.55
LlH Orifice Pressure Drop In H,O 1.153 1.133
y Meter Calibration Y Factor dimensionless 1.001 1.001
Vm Volwne Gas Sampled--Meter Conditions cf 353.940 348.645
Tm Avg Meter Temperature "F 88.2 86.4
..J!lP Sq Root Velocity Head Root ln. H20 0.7627 0.7748
w~c Weight Water Collected Grams 371.5 387.9
Tt Duration of Test Minutes 480 480
cp Pitot Tube Coefficient Dimensionless 0.84 0.84
Dn Nozzle Diameter Inches 0.2240 0.2240
C02 Volwne% Carbon Dioxide Percent 1.80 2.00
02 V olurne % Oxygen Percent 17.20 17.20
N2&CO Volwne% Nitrogen and Carbon Monoxide Percent 81.00 80.80
Ymstd Volwne Gas Sampled (Standard) dscf 280.391 277.653
Vw Volwne Water Vapor scf 17.516 18.289
B W s (measured) Fraction H10 in Stack Gas (Measured) Fraction 0.059 0.062
Bw, (saturated) Fraction H20 in Stack Gas (Saturated) Fraction 0.110 0.119
Bw, Fraction H20 in Stack Gas * Fraction 0.059 0.062
xd Fraction of Dry Gas Fraction 0.941 0.938
Md Molecular Wt. Dry Gas lbllbmol 28.98 29.01
M, Molecular Wt Stack Gas lbllbmol 28.33 28.33
%1 Percent lsokinetic Percent 100.8 98.7 AVG
T, Avg Stack Temperature "F 111.2 113.8 112.5
A, Stack Cross Sectional Area Sq Ft 0.887 0.887
Po Stack Static Pressure In H2o -0.750 -0.750
PbP Sample Port Barometric Pressure In Hg Abs 24.43 24.48
P, Stack Pressure ln. Hg. Abs 24.375 24.425
Q, Stack Gas Volwnetric Flow Rate (Std) dscfin 1.88E+03 1.90E+03 1.89E+03
Oa Stack Gas Volwnetric Flow Rate (Actual) cfin 2.65E+03 2.70E+03 2.67E+03
vs Velocity of Stack Gas fj:nn 2.99E+03 3.04E+03 3.01E+03
Curies Radionuclides per sample pCi 23324.6 22451.8
Crad Concentration of Radionuclides pCi/dscf 83.186 80.863 82.024
ERrad Emission Rate of Radionucbdes pCilhr 9.378E+06 9.221E+06 9.299E+06
* If the measured moisture content is greater than the saturated moisture level (supersaturated),
the saturated moisture value will be used in all calculations (40 CFR 60, Method 4, Section 12.L7).
Dryer Baghouse
TABLE V
COMPLETE RESULTS, PM
DENISON MINES CORPORATION
YELLOW CAKE DRYER BAGHOUSE
Symbol DescriEtion Dimensions Run #I
Date Date 4/4/13
Filter# XIOO
Begin Time Test Began 9:50
End Time Test Ended 11:54
Pbm Meter Barometric Pressure ln. Hg Abs 24.55
~H Orifice Pressure Drop In H,O 1.594
y Meter Calibration Y Factor dimensionless 1.004
Vm Volume Gas Sampled--Meter Conditions cf 96.458
Tm Avg Meter Temperature OF 76.8
-~~p Sq Root Velocity Head Rootln HzO 0.8216
Wl:wc Weight Water Collected Grams 10.4
Tt Duration of Test Minutes 120
cp Pilot Tube Coefficient Dimensionless 0.84
Dn No=le Diameter Inches 0.2215
C02 Volwne % Carbon Dioxide Percent 0.00
02 Volwne % Oxygen Percent 20.90
N 2 &CO Volume% Nitrogen and Carbon Monoxide Percent 79.10
Vmstd Volume Gas Sampled (Standard) dscf 78.533
Vw Volwne Water Vapor scf 0.490
Bws Fraction H~O in Stack Gas Fraction 0.006
xd Fraction of Dry Gas Fraction 0.994
Md Molecular Wt. Dry Gas lbllbmol 28.84
M, Molecular Wt, Stack Gas lbllbmol 28.77
%1 Percent lsokinetic Percent 100.8
Ts Avg Stack Temperature OF 96.3
As Stack Cross Sectional Area Sq Ft 1.396
PG Stack Static Pressure In_ H20 -0.41
PbP Sample Port Barometric Pressure ln. Hg.Abs 24.48
Ps Stack Pressure ln. Hg. Abs 24.450
Os Stack Gas Volumetric Flow Rate (Std) dscfin 3.39E+03
Oa Stack Gas Volwnetric Flow Rate (Actual) cfin 4.39E+03
vs Velocity of Stack Gas fjJm 3.15E+03
Curies Radionuclides per sample pCi 87350.0
Crad Concentration ofRadionuclides pCi/dscf 1112.2698
ERr ad Emission Rate ofRadionuc]ides pCilhr 2.261E+08
Symbol
Date
Filter#
Begin
End
Pbm
~H
y
Vm
Tm
,j~p
Wiwc
Tt
cp
Dn
C02
02
N2 &CO
Vmstd
Vw
Bw,
xd
Md
M,
%1
T,
A,
PG
PbP
P,
Q,
Oa
v,
Curies
Crad
ERrad
TABLE VI
COMPLETE RESULTS, PM
ENERGY FUELS RESOURCES, BLANDING, UTAH
GRIZZLY BAGHOUSE
DescriEtion Dimensions Run#1
Date 6/5-6/13
Xl32
Time Test Began 15:40 6/5/13
Time Test Ended 11:48 6/6/13
Meter Barometric Pressure ln. Hg. Abs 24.35
Orifice Pressure Drop ln. H20 0.940
Meter Calibration Y Factor dimensionless 1.000
Volume Gas Sampled--Meter Conditions cf 323.044
Avg Meter Temperature "F 76.1
Sq Root Velocity Head Root In H10 0.2453
Weight Water Collected Grams 27.1
Duration of Test Minutes 480
Pi tot Tube Coefficient Dimensionless 0.84
Nozzle Diameter Inches 0.3808
Volwne% Carbon Dioxide Percent 0.00
Volume% Oxygen Percent 20.90
Volwne% Nitrogen and Carbon Monoxide Percent 79.10
Volwne Gas Sampled (Standard) dscf 259.668
Volume Water Vapor scf 1.278
Fraction H,O in Stack Gas Fraction 0.005
Fraction ofDry Gas Fraction 0.995
Molecular Wt. Dry Gas lbllbmol 28.84
Molecular Wt. Stack Gas lbllbmol 28.78
Percent Isokinetic Percent 94.1
Avg Stack Temperature "F 90.6
Stack Cross Sectional Area Sq Ft. 1.917
Stack Static Pressure h1 H20 -0.035
Sample Port Barometric Pressure In Hg Abs 24.32
Stack Pressure In Hg Abs 24.317
Stack Gas Volwnetric Flow Rate (Std) dscfm 1.39E+03
Stack Gas Volwnetric Flow Rate (Actual) cfin 1.80E+03
Velocity of Stack Gas !pm 9.37E+02
Radionuclides per sample pCi 125.1
Concentration ofRadionuclides pCildscf 0.4817
Emission Rate of Radionuclides pCilhr 4.028E+04
Grizzly
General Nomenclature
%1 = percent isokinetic, percent
A,= (0,2 I 4). TC
ASt.P = see --Jt.P
Btu= unit heat value (British thermal unit)
Bws = fraction of water in stack gas (may have designation of "measured" or "saturated")
"measured" represents measured moisture based upon sample volume and water collected
"saturated" is a calculated value based upon stack pressure and temperature
C0 = average of initial and final system zero gas calibration bias checks (ppm, percent)
Cavg = average gas concentration (as measured)
C8 = concentration of particulate matter, back half(gr/dscf,lb/dscf, etc.)
ccond = concentration of condensibles (grain/dsct)
Ccors = concentration of coarse particulate (gr/dsct)
C0 ;, = measured concentration of a calibration gas when introduced in direct calibration mode
Cra = concentration of particulate matter, front half, actual stack flow (gr /act)
CF = concentration of particulate matter, front half (gr/dscf,lb/dscf, etc.)
Cgas = Cavg corrected for initial and final system bias checks (Equation 7E-5)
Cm = average of initial and final system upscale gas calibration bias checks (ppm, percent)
Cma = actual concentration of upscale calibration gas
Cmetal = concentration of metals (ppm, 11g/fe, etc.) atomic symbol replaces "metal"
C02 = percent carbon dioxide in the stack gas
cp = pitot tube coefficient (0.84)
CPMlO = concentration ofPM10 particulate (gr/dsct)
Crad =concentration ofradionuclides (pCi/dsct)
CS = measured concentration of a calibration gas when introduced in system calibration mode
Cx = Any species symbol may replace X. Units may be expressed as ppm, lb/dscf, etc.
Cx (corr) = actual gas concentration corrected to required percent 0 2
Curies = Measured radionuclides per sample. Units may be pCi or uCi.
De= jet diameter (em)
D/F = Dioxins and Furans (See laboratory report for D/F descriptions and nomenclacture)
t.H = orifice pressure drop (inches H20)
t.H@ = orifice pressure (inches H20)
t.Hd = orifice pressure head (inches H20) needed for impactor flow rate
Dn = nozzle diameter (inches)
t.P = stack flow pressure differential (inches H20)
Dp50 = 50% effective cutoff diameter of particle (em)
D, = diameter of the stack (feet)
EA = percent excess air
ER8 = emission rate of back half particulate (lb/hr)
ERcond = emission rate of condensibles (lb/hr)
ERcors = emission rate of coarse particulate (lb/hr)
ERF = emission rate of front half particulate (lb/hr)
ERgas = emission rate of a gas (lb/hr)
ERmmBtu = emission rate per mmBtu of fuel
ERPMlo = emission rate ofPM10 particulate (lb/hr)
ERrad =emission rate ofradionuclides (pCi/hr)
ERx = emission rate of compound which replaces X. Units are usually in lb/hr.
F0 = Dry based fuel factor. Ratio of the gas volume of the products of combustion to the heat content
See 40 CFR 60, Appendix A, Method 19, Table 19-2 for fuel factor values.
Kc = Cunningham slip correction factor
'A= mean free path of molecules in gas phase (em)
mmBtu = million Btu
General Nomenclature
Mcond = mass of condensibles (milligrams)
Mears= mass of coarse particulate (milligrams)
Md = molecular weight of stack gas, dry basis (lb/lb-mol)
MF = mass of particulate on filter (mg)
Mpp = mass of particulate matter on filter and probe (mg)
mmBtu = million Btu
Mp = mass of particulate matter in probe and front wash (mg)
MPM!o = mass ofPM10 particulate (milligrams)
Ms = molecular weight of stack gas, wet basis (lb/lbmol)
Mx = mass of species "X". Units may vary and other descriptive subscripts may apply.
1-ls = gas viscosity (poise)
Mwx = molecular weight of gas species (g/gmol)
N = number of jets per plate
N2 = percent nitrogen in the stack gas
0 2 = percent oxygen in the stack gas
-.Jtu> = average of the square roots of LlP (may also be referred to as ASLlP)
-YllP1 = square root of LlP at point 1 of the current test, Method 201A
-YllP1' = square root of LlP at point 1 of the previous traverse, Method 201A
-YllP'ave = average of the square roots of tll' from the previous traverse, Method 201A
Pbm = absolute barometric pressure at the dry gas meter (inches Hg)
PbP = absolute barometric pressure at the sample location (inches Hg)
Pa = stack static pressure (inches H20)
Ps = absolute stack pressure (inches Hg)
Pstd = absolute pressure at standard conditions (29.92 inches Hg.)
e = time oftest (minutes)
81 = sample time (duration in minutes) at first sample point for Method 201A
8" = sample time (duration in minutes) at sample point "n" for Method 201A
81est~ target test time for Method 201A (minutes)
Q. = stack gas volumetric flow rate (acfm)
Os = stack gas volumetric flow rate (dscfm)
Osc = actual gas flow rate through the cyclone (acfm)
actual gas flow rate through the impactor (acfm)
wet stack gas std. volumetric flow ere/min, wscfm)
gas constant (21.85 inches Hg*ft3/(lbmol*R))
particle density (1 g/cm3)
Ps = stack gas density (g/cm3)
Tm = stack temperature (°F)
Ts = stack temperature (°F)
Tstd = absolute temperature at standard conditions (528°R)
Tt = Duration of test run in minutes. Also see 8
Um = mean molecular speed (cm/s)
Vm = sample volume (ft3) at meter conditions
Vmstd = volume standard (dscf), sample volume adjusted to 68°F and 29.92 inches Hg.
Vs = velocity of stack gas (fpm)
V w = volume water vapor (set) at 68°F and 29.92 inches Hg.
Wtwc = weight of the condensed water collected (grams)
xd = fraction of dry gas
Y = meter calibration Y-factor (dimensionless)
\jl = dimensionless inertial impaction parameter, 0.14
General Sample Equations
%1 = Vmstct o (Ts + 460) o 1039 I (8 o Ys o Ps o Xct o D/)
As= (D/ I 4) o 1t
Bws = V w I (Vmstd +V w)
CB = MB o 0.01543 I Vmstd
Ccand = Mcand 0 0.01543 / Vmstd
Ccars = Mears 0 0.01543 I Vmstd
Cra = Tstd o Crp o Ps o Xct I [Pstd o (Tm + 460))
Cr= Mrp o 0.01543 I Vmstd
CPM10 = MPMIO o 0.01543 I Vmstd
Cract = CuriesiVmstct
Cgas (carr)= Cgas o (20.9 -desired %02) I (20.9 -actual %02)
case Dp50 = ...J [J.lS 0 \jf 0 N ° 7t 0 D/ 0 18 I (Kc 0 Pp o Qsce o 4))
0 2091 0 7091 PM" DPso = 0.15625 o [(Ts + 460) I (Ms o Ps)J o (!lsI Qsc)
ERcand = Ccand o Qs o 0.00857
ERcars = Ccars o Qs o 0.00857
ERF = Cr o Qs o 0.00857
6 ERgas = Pstd 0 Qs 0 Mwgas ° Cgas 0 60 I (R 0 Tstd 0 10 )
ERgas = Cgas(lb/dscf) 0 Qs 0 60
(Either ERgas equation gives equivalent lblhr values to 3 sig. figures)
ERmmBtu = Cgas(1b/dscf) o F d o (20.91(20.9 -%02), Method 19 Equation 19-1
ERPMIO = CPMIO 0 Qs 0 0.00857
ERract = Cract 0 Qs 0 60
Kc = I + 2 o A o 1.257 I DPso
A= lls I (0.499 ° Ps 0 Um)
Mct = C02 o 0.44 + 0 2 o 0.32 + N2 o0.28
Ms = (Mct o Xct) + (18 o Bws)
J.ls = [51.05 + 0.207 • {T, + 460) + 3.24 •10-5 • {T5 + 460)2 + 0.53147 • %02-74.143 • Bws] • 10-6
Ps = Pbp + (PG I 13.6)
81 = (...Jt-,.Pl' I ...Jt-,.P'ave) o (8test I pts)
en= 81 o ...Jt-,.pn I ...Jt-,.p1
Qa = Ys o As
Qs = Qa o Xd o Ps o Tstd I [(Ts + 460) o PstctJ
Qsc = [(Ts + 460) 0 Pstd I (Tstd 0 Ps)J 0 [(Vmstd + V w) I 8]
Qsce = [(Ts + 460) o pstd I (Tstd o Ps)J o [(Vmstd + Yw) I 8]
Qw= QsiXct
Ps = Ps oMs o 3386.39 o 10-6 I [R o (Ts + 460) I 1.8]
Um = 100 o ...J {[R 0 (Ts + 460) I 1.8 ° 8 ° 103] I [1t 0 Ms]}
Vmstct = Vm o Yo Tstct o (Pbm + t-,.H I 13.6) I [Pstct o (T m + 460)]
Ys = 85.49 o 60 o Cp o ...Jt-,.p o ...J [(Ts + 460) I cPs o Ms)J
Yw= Wtwc 0 0.04715
Xct = I-Bws
APPENDIXB
South Yell ow Cake Scrubber
Preliminary Velocity Traverse and Sampling Point Location Data
Field Data Sheet
Yell ow Cake Dryer Baghouse
Preliminary Velocity Traverse and Sampling Point Location Data
Field Field Data
Grizzly Baghouse
Preliminary Velocity Traverse and Sampling Point Location Data
Field Field Data
B
South Yell ow Cake Dryer Scrubber
Preliminary S Y Cake Serb
I
Facility Energy Fuels
Stack Identification South Yell ow Cake Dryer Scrubber
jA Date t1vZr( l
--
N Barometric Pressu.-e
Pbm in Hg PbP in Hg
B -1 Static Pressure (P0) in H20
Estimated Moisture (Bw.) 4-6 %
Sample Height from Ground 70 feet
Comments:
Stack Dia 12.75" Reference: 0"
I' Ports are 7' Upstream from next disturbance
Ports arc 30' Downstream from last disturbance
Traverse Percent Distance From: Ports
Point Diameter ID Reference A B c D E F
1 6.7 0.85 0.85 t<>s--,.-lr1[ .s-o .• n
2 25.0 3.19 3.19 Jl)~ /d'5 ·f>-c, ' r1'"
3 75.0 9.56 9.56 lo'f-I <> fr'
·II} . (; ~
4 93.3 11.90 11.90 I" C. .c,o( /l)<"j . (1':>
•
Averages:
Ts ___ _ LFlow ----
~P __ _ --JM ----
KEY=>
_____ Field Data Sheet
..(OD)~ -._ ~IfTCO Filttr~'-""Sampl~ BQX_Q:_
Location: SouV,a;ellow Cake Dryer Scrubber
Operator: ___ ;~.,..,-------
DGM aP II AH (in><,Oi II Vacuum 'I Temperatures ("FJ 11 OQMicmp(T.,) 1 I Probe I Probe out I Oven I 1 Traverse jj Ti~e . !J
Mm (8) {ft)) Out In Point
0
2.0
YO
2 bO
2 ¥0
2
3
3
3
4
4
4
1
1
2
2
2
3
3
3
4
4
4
I of+ Run#. _\ Page_ -
-
A I .o N
Stack Diameter 12.7 5" Port Reference _,QL'_' __
7' Upstream from next disturbance
30' Downstream from last disturbance
Assumed Moisture 4-6%
Probe ~1-(p Cp 0.84
Nie ribrat~o.:' .1 ..,I ..f , t -~ .u \ . -z.,t,.-
AvgD. • Z.~J in-:;;:----
Gas Bag 'H -())
Console-5'-
Y-Factor [· Otl} AHil!l~inH,O
Barometric Pressures
Pbm. -1..'··(.· )0 __ in Hg
Pb z--/.'i.> inHg
p --J_ ,..--'y-1'0 (, •-~ , inH20
"'"" 7 Leak Check' Pre
tt'imln_ ():. 9-D_ (p
vae'" Hg--.:?:. l _
PitotRote o-0 -... ...!...
lnH,O -~ :L
o -oo3 rz:-
()-()
OZ-r.r
J 7 ~r-g
t..(& () min
Total -~5") qtf() '£-~-~~-'2.1P(lif / ~~
Water Collected
Time Sampled
Review ~
Average ".1~-z,t \.\G"3 l \\-v
Additional (Extra) Leak Check Information I _:=l_[)GM__before Leak Checlt__~c ("Hgl_ ( R~tte_ (_!t~lrtiifli]L DGM After Leak Check
'B"~. 0
I Vac ("Hg) [ Rate (fetmin)
K"'
K "'
@Tm
@Tm
'-'I J.,~J ' I ~
.; ' . Field Data Sheet
Plant: Ener:y F~~s\
Date r{lf\ J.~
PoUlt
Traverse lj Time I
Clock I Min (9) I
1
DGM
(ft'J
);ETCO ?
Filter,_ ~~ SampleBox_k-Page __ \ _of-+-Run # _ -z_.
Loci!tion· Sou er Scrubber
Operator: -,
cu. HPl II Desired I Actual
~p I\ ~H c:n><,O) II Vacuum II 1 Te":peratures \..-' 1 1\IXl~ Tf'l'(T~J
(U.Ho> 11 Stack (T,) I Probe I Probe out I Oven EffiuentH Out In
i Bo N
1 Stack Diameter 12.75" Port Reference~O'_' __
2
2
2
3
3
3
4
l'iU ~ {p()V. S't:J~~l.I3JITT'1l l· Ccfll ? ~· fl1-: l E--:'-1-Ph..Jt~ I '2-'{O I 5-~11 ?j-cjj_q 4
~~~ o II (p 1, 1,. \ ~ q ~, tf CJ .!1-01-; I. q "7' L 'Jlf l (1/ff,;'J-I 1--z._IR f l1--v\. I I 5'9 rw-11 11-
t s-o 1lr~'Zio-.9'i'DJi l'~ IU~QZ.,..[i~~-11 -11 v 11» ~T-1.1, ~\lilil 0 I<;;;·~ 0.1 c; ~ _Lll _ [~oau~o -~ 1 ~J~C?.-~T!~TnJ-~-~~ ~ -\1 =71 ~y~ zct~~'[~~~5(~l@<k·I J oD
4 I z.z. {pflt;. (;7/~1 --5 t /-o ~ h.o<£ lf. lr'L-1:--l~ L(2 z..~S :7 , "'! '1
1 11 lL.·~-v 1 z~ 0 ~G~~-6 .L{ 33[-&F li7Tu I EI1JC3JC 1CLl~?;~ni-1.5St-f.t:z/(l ~ 51'11 ~\P. I '1 4
z&0 ~ &~q_r~~~<-\J,fg,\ 11\.lt, -ll.f(_,~ ~II \t( I ?_4.~f;51t-"7llrnflll <t10L~&.
1 z.FII.J"oq_ Ob'1J["kYIT1f!l7 .i:;,l_KJI trlo I 'l"o/}-z.~z.-17_ -s-r 1.;-~11 <r5'"rc:r~
2 13 V 0 lt'TI~ -1'7TI~ll r-:-vrrl~"ilill~-~~--~ ((J h/ ~..tq Ttlf-fli?)'lc; t) r~:;J '11-
2 7t (? 11~q o.ttJ"v-11-t-; 111 -1.D h. L o 1r ~fl\ C) FzA\< lt5to 1 'J 0'fk q ~ ~<;J-~ 5"
2 Ytl711 ~~7. C-F'\ -~~&-~ Jl t -1-i JJ ... i-'ill..s=.J[IL!;?_ t.'7l2JZ.~~ L1:~\T5_>n~, I q ~'
3 J&OII1-1'V ·~~'li!I,..<J-&II .-"1 '11: ~qll q-11 11\e li"7~ ft'{(fj--:;z:-')1{ s-'fT~cf I OJ Lf
3 ,yo II 1-~tt-:-t7~~-~tlC"~'l.l .q ~·11_5 II Wt I7~YDT ~ L 2'7)1 ~~~rg-~l -'1 ~
3 "Wlf~W-7..711-{;-:} 11 l-1-Y I t~t CS'Ju ll-5-~.ft Lw'J -z':!]A.1·1 s:-2 I q :7
4
4
4
Total
Average
I
41-u II ~r 3 ·~-s--o. II -1lP I ·tt t1l "'7.1 'W l1,~.'k i1:1PS" 11}-f) ~~--'tfs--0 1 f1lP ~<~0 11 q~_'tf~~ILJl[(. i&L1ti[~JI__li_CP 1 ·7,'-\v I ~z.:5"UI1.-q\ I~+ l~lcro'
lito II ~O .V'')~~-{,(! ll l:tli 1(.-z,[~l ~U -rn~ll.-~1 17 .. Cf'1 &-{ i l 5-~II S"fo [ ~1
r.t~0 ll ~S(/)_qqc;
")-il '6 .(J ~ :; .J \ ~-. 5'1'1 t-" t f i ~ -
.J • 11-~S' t. \7)
~1-)t --
\ t;.g
t.{/ '11-
g~.~
Additional (Extra) Leak Check lnfonnation
I OGM before Leak Check I Vac ("Hg) I Rate (te/min) II OGM After Leak Check I Vac ("Hg) I
7' Upstream from next disturbance
30' Downstream from last disturbance
Assumed Moisture 4-6 %
Probe '2 1"(::, Cp 0.84
Noi'e ilibrat.!_O.!_l . 1 _,{ ..{ ~ t. -~ • .z:t, \ • ~
AvgDn • Z. z..o--j l~h~ ---
Gas Bag z; -0 3
Console->":-
Y-Factor / • 0 4 }
a~ /. '( ~ hn H~O
Barom:n-i~ P~~S
P.bm _ '2. '-{ '"S __ in Hg
PbD _ Z <-{ • t.f 16' r Hg Po-c.o ·1:~ nH20
Leak Check: Pre f" 1 Post
ft'tmin 0 .QO 7 0 .oo'1
vac in Hs-"l. :~·-=• f -z_....-
Pi tot Rate 0 · 0 -..• .L..
InH10 -q. ~
o.o
~
Water Collected ~ & 1 . CJ g
Time Sampled_ ru 0 min
Rate (fetmin)
Review I ·
K«
K=
•
@Tm
@T,.
Yell ow Cake Dryer Baghouse
Prelim 6 pts blank
I
Facility Energy Fuels Resources, Blanding, UT
Stack Identification North Yellow Cake Dryer Baghouse
Date '-11411)
l Barometric Pressure
B Pbm Z.~.)) in Hg Pbp l~ ,"ff! in 1-lg
N 0 Static Pressure (PG) ~ .jl in H20
A Estimated Moisture (Bws) 1 %
Sample Height from Ground feet
Comments:
Stack Dia. 16 Reference: 0
Ports are 57" Upstream from next disturbance
Ports are 468" Downstream from last disturbance
Traverse Percent Distance From: Ports
Point Diameter ID Reference A B c D E F
1 4.4 0.70 0.70 ~,.._1{1
2 14.6 2.34 2.34
3 29.6 4.74 4.74
4 70.4 11.26 11.26 'll 14
5 85.4 13.66 13.66
6 95.6 15.30 15.30 "fl. It/. 'l.
1-
Averages:
Ts LFiow --------
L1P ..JL1P --------
KEY=> ITs
Sftl"'( Field Data Sheet
TETCO
Filter)(: i~O Sample Box~ . . ~-\-~_~_~# __
Plant: Energy Fuels Resources, Blanding, UT
Date: '1{ -{( J 3
Traver5c Time DGM 6P
Po tnt Clock Min(B) (n') ti.111u)
1 c:r. fb 0 4'11 Z.{?-·~4
2 10 li"il. olfo ·11
3 lO '1 { I • 310-.< • C..'1-
4 30 "lf'<.•.no ·81.
5 <{Q 'i~B. r&o ·83
6 50 '{1-1:..~00 .ao
1 r.J:.5<( "o .. ,e{ .. o{)b I ,"f' -2 10 4 '( ,..,olro •Si
3 So 5oZ.~3o ·8o
4 110 51i."i<t1 ·91Q
5 too S'lO. ~'K •18
6 110 S':Zel\ I 30 •11
n;sc.t ~2.0 s:n·.,fo
-
.!!.H fi1H20) Vacuum
Desired Actual (i.llll)
·1S o6 1-
1"34. ''>If L.
1.1~ 1.-{J '"(
I·~S I. ~9:, 'i
I·~ I·~ I.{
I• it. I.~L ~
,,.1\ l.1( ~\
u04 l.~ '1
l.g·z.. I .8"2.. 4
l·OO z.oo '-l
(.11 1.11 'i
1•7-) h1f "{
Total 9(,·~~B .,r'jJoS'\l / \ct.r~v
,L .... L .. 0 -~1..\l, \ . 54.'{
Comment;: Time BsghousoAP Time BagllouseAP
jO·.~~ ~.1, n:o1 e.-r
.o -~( 1 .\ ll'.l,( q,.,
fu:-t{ ~·lr \t' .• ,( <:;..1-
---
Location: North Yellowcake Dryer Baghouse
Operator:~ M. A ~~(c-
Temperatures n>
Stack(T,) Probe Probc:<M Filter
'ii I'.X~ tl,.} l.!. ~
9(, 7_(.,1. u.> "C.~ 3
'1~ ').3o z.t:. I ~~...,
'1(., l7o l1"1 2-li
Gfjg l<..i 2n zTi
'1~ t :n zr~ l{C(
"\~ z.s·~ ,.,.g H8
Cf{# l(,b ZioO 2.(,0
'j(, z..3o l{~ 2.1)
tt:r 2.'-l) 2,;~ H'f
q~ Z..'fo z. t.'t ~C..'{
ors Z.S\ l5'f Z~C(
l\ScP/
q~.; -
Effluent
57-
'ito
tlf
!..j(
'fl-
4~
So
..S'i
5'5
5~
5$?
(q
OGMTtmp(T.J
Out In
~,·-1 t..f
{.,~ &:}
~f 4>3 eo :or
~3 (:.8
'B":t-~~
B> 't~
~€! /J
~Q 11
~ 13
q., 1~
~' 18
i8 ~)11'
l(# .~
i 8 Ao N
Stack Diameter _16" __ Port Reference _0.0"_
Ports are
Ports are
~Upstream from next disturbance
468" 00\>11stream from last disturbance
Assumed Moisture _ ___:. __ %
Probe lliJt Cp~
Nozzle Calibration
.U.I ,zz.t t l.l'Z.. I "tl Z. -----
Avg D. ' Z. Z I ( inches
Gas Bag Ambient Air
Console ~Gf
Y·Factor (.oo"i
hH0 \ . (, 1 'I in H,O
Barometric Pressu!Ss
Pbm Z q ,{) inHg
Pb. l. <{ ' 'i ~ in Hg
P -# ijfu..-• o.ll in H,O c.__ .
L<:>lo. Chock: fu.
fi'lmin 0 • Q:>Z..
vac in Hs Z. Z •'0
faa
~
ll.:Q
Pilo!Ra!e 0·0 _Q:.
~~,H,O f2·0 ____l:_Q
Water Collected I 0 • '-{ g
Time Sampled \ 2.0 min
Review ~~
K-@1; ••
·~ .,...""
1-~~~J~\~ r ·" (e~ fo J
Grizzly Baghouse
Prelim 12 pts blank
Facility Denison Mines
Stack Identification Grizzly Baghouse
Date (p( 5·b[/3
l Barometric Pressure
Pb111 z 1/.j:) in Hg PbP 2'-/,3 2: in 1-lg
N AO B Static Pressure (Pc;); oJj-in 1-120
Estimated Moisture (Bw,) I %
Sample Height from Ground feel
Comments:
Slack Dia, 18.75 RelcJcncc: 3.0 Must use 36" probe or lon,ger to keep box outside handrail
Ports arc 24.5" Upstream from next disturbance
Ports arc 48" Downstream from last disturbance
Traverse Percent Distance From: Ports
Point Diameter ID Reference A n c D E F
1 2.1 0.50 3.50
2 6.7 1.26 4.26
3 11.8 2.21 5.21
4 17.7 3.32 6.32 I
5 25.0 4.69 7.69
6 35.6 6.68 9.68
7 64.4 12.08 15.08
8 75.0 14.06 17.06
9 82.3 15.43 18.43
10 88.2 16.54 19.54
II 93.2 17.48 20.48
12 97.9 18.25 21.25
! I
Averages:
Ts L Flow ----
L\P ~L\P --------
KEY=>
-----Field Dara Sheer
Planr. ~> f."\~f~~ Fv ~l.S
o,ue: r.J 5 ' f.; / J)
TJ.:l\l(fSC T•me DGM aP 6H I..,H:CI
Fo•'' Clock Min (9) 11 "1 , .. JJ 0• Desired Actual
~-5· ~}e. 1 1 5:~ 0 1 ~3. ~Z.'O 'o<4> .'04 .~t.{
2 lO :n"-1C:O' .oi.J) r'&. • '0 (,
3 40 3~'1-IB~ 'o55 \ .ol I-~ t
l:,o 3(,;~' {'-IQ .. ~s~ _,. ' / 4 I ·OJ I .Ol
5 BO 37/.'l,Zf , O)Q I~~ i .o'\
~ !OO . 3<il. ~i) .. o"c t. 0"\ j.0'1
12.0 i.!o-'· \"o 'ot>2.. i -1 ~ { -13
1'{0 t..i2.0 -'1)D . o)~ l·olc 1-o!.?
1 ~0 t.p,), 190 , o)O, 1-0+--r. o=t
1~0 '-l<-19.~'-J .a)(o t-o£.. I oz..
11 loO q"3 .\, g:) .o53 • q':7-,qf.-
12 !<J::...io uo l.lf/. oz.-o lo:n 1· Oi) i.o0
L.-C.-1,.. 1 ,:38 ~'-iO '-!«-1.<-n .... •"'"il· .._g"f .~I{
2 2'-0 50'{, ~20 .o'i'i} .~ .9=\
3 z.so sn. "?>9o • o'(@> ·W? I Bq
53o.~l. ~ 4 3co t::.,_l. ~ .o;)Q ''fl.. .~z.
-+1 3z.O 5'1'-i.o"v .o~_ . q{? ,'fS
340 !"51. 5'3{ • e-5) 1.oo L'VO
33 3 "0 5 i-\.c. ~a ,o'i'{ • Be ·SO
3'i!O 56'-1-31{ • o'{!p ·Bii . 8~
' ~oo 5'f/.l'i ( • otj!.., .<34: ·~N 9
10 4to {..oc:t.Cfo{ •o'i3 ·18 ,,~
11 'i_lfO &l2. ')Z{ • ~'i~ . ao .so
12 !.{leO {,_. 3'-i 1!0 .1!'{) • g-z. I '82..
tL :tt B 1.{00 ~q~. SS)
Fil•eri..IJC.... TETCO ---Sample Box ~
Va~;uum
t'" H~)
t.,..
L
L
-z..
2.
~'--
L-..,
'-
'2...
2-
7-
"'l..
1.
2-
2-
2-
'2-
(_
'l...
2-
"2...
2-
2--
"2-
Location: Grizzly Baghousc
Operator: f•(\. M~Nu.A{0-,_\0...,
Temperawres (FI
Stack [T,) Probe Pr.Jb1;0u1 Filler
'j lo z -o ~-U.J 'Z.h)
'?2-1&V ZC:,) lbJ
G}(o? 7..51--lift lb'i.
<11-ZIO z;~ l)Jo
C\8 z... .... h1 lb~ l(:,~
q-·+-' -., C::J.:, 2'5''+ 2. i .:r-
q~ u .. { 2~' Zb !
Cj(o ?.Z) zr I "lfl
q~ z. ii B ?.. ["z._ z..;t...
_!1<.{ l'-/Cf . 2_(0 25'0
0!<-1 . Z.P z...c=.)·1 z.br
~:z.. no· Zik z.;0
"1}... 250 Zi:lt U.<t
18 '2.<..0 2 "fo Z.fO er g.~ l.i zi-=
8~ l.C,5 2.19 -,-c. ~:> j
'0) l,b) 2..'-''-1 l.."4-f()~ z_ro-:r 210q W·~
f3B 2C6( 1. -{) 2. ,. ' l ~
~0 Z,G,( Z.'-('1 ?.'lq
G1 ! 271 z;~ 25~ cu . lG,-( lS-=t-251--
'tl. 2. (, 5 z.O U.3
q:J Z.3o '2,(.f\{ 'Z.4'i
DGM Tern~ (T.l
F.illuenl Out In
~a..J ~~ 7~
~1.. /<{ 11
"~ -.u ' . 1'8
I. d r.p. l(, _90
50 7{.p Q,l
{;,1) f-7-f]2.
b f T-r 'aL
"3 ib 62.
b3 ?r.:. 3 t
(o3 {(,. Bl
(..,I l) n'O
I.. G. j) "7'1
5~ ~-=t-(pi-
S"l 70 73
5Z "73 /(...
5.3 1'-! 7~
55 I[ 1Cf
5-:r-{!;e. so
'i~ l7 <(j(
l.{f; 13 /:)
'-{9 -,-) 19
~2-I~ lq
53 75 7_!
53 b'r 72..
Pagc_i_oi~ Run #_j__
j AOB N
Stack D•,;mer~r 18.75" Port Reference ___l.Q::__
Ports are 24.5" Upstream from ne~t di~lurbance
Ports ar: 48" Downstream from last dostllrbanec
Assumed t ... 1uisiure
Probe 3gb ----~0
Cp ~
Nozzle Cal1bration
t3€tC 13"e l ·'3€{ .381
A'g D, .3~o e, ir.ches
Gas Ba£ Ambient Air
Console~
Y-Factor l . 000
.c.H@ 1 . 'lCj0 in H,O
BarometrlC Prc:ssures
Pb., Z'l .){' inHg
Ph 2. '1-)-z_ in H~ ,. -
p -· O~f' inH.O 0 •
l~ak Check· ~~ Pfe
n"/rn:n 0·00 l..
...... ~ 111 Hs Z Z.. .. -o
P1:o1 Rat~ 0 .. ()
lnH:O~~ r' •7..-0
Po~t
~z...
11.-0
'J.O
,_pr,' I.J]lk
' z,-{
Water Collected 't l· l ~
Time Sampled '-{SO mm
Tot:. I 3 Z 3. o'i'-{ ..; s. roS'i;) ./ 1.:z. -55 v I \1 ( ./ 3~54 / Rr:\•ie\v t_~--''-------
Average
Comml!ni.S
..J '-z..t..~{-z.. • '1 'io
R(J....<\ f'~r-+-c 4.\....(t../1r/~:;z..3.:'1..e
oo,M' , .. -r·\\"') (1'.'-j;o,c..c..n y .:Jf .... I ''D I • . ' p. '\.
¥-."'-'\ <~'I,-(';;., L\\., (
\J~iV\·. \S'j ,q)\
, I , s~ I"'( f /; (., f J I I '1, • •t "\ . ,. l {,.
t b, \ ../
(;(\ ~a·n·SB)
C(o,(..
51-vi-d.O..Ji'l @_ ll'.ol
~e,)~c+--9 \LH
!]e.U.. ,{0+ t¥f-•r.r-•
j2~k. s j..u(.ll-)I'\
~;z)-l-'
I lo, I
!.. a a. .(. (4£_!.(.. ?<>( t P.
ilrt..
1.\ l.A""-0 . c-o 'L -
1..1--0·0 ?:tlLi--~ ~
·~ ')
K=
K=
@Tm
@Tm
.Po~+-
0-0C"L
p ..
o.O
--::::< ~ ~r . "!.J .
South Yell ow Cake Scrubber
Sample Recovery
Gas Analysis Data (ORSAT)
Yell ow Cake Dryer Baghouse
Sample Recovery
Gas Analysis Data (Ambient)
Grizzly Baghouse
Sample Recovery
Gas Analysis Data (Ambient)
Chain of Custodies
Lab Analysis
APPENDIXC
c
South Yell ow Cake Dryer Scrubber
METHODS
Facility: Denison Mine Date: --------
Stack Identification: .:..N..:...Y:....:C:::....:::.S.:..:cru-=b::..:b::..:e..:...r -------------
IMPINGERS
IMPINGERS
IMP!NGERS
------------
Run: r Sample Box: {)
Thtpinger Number
6
drop out
'
Total (g)
Run: 2 Sample Box: D
lmpinger Number
..1.. I 3 I 4 I ....!.. 6
Initial Volume ofliquid fl'ltO) in impiugc:rs. (ml)
drop out Silica Gel
I
Final (g)··-=-..:~--+--:__-~_...;...,.-"-~"-~1.£."'--I-;;......;:...__1--1-=--....L....
Initial (g) So\ ./
Net (g) It';>,
Run:
I -
drop out
Sample Box:
l:rger Number
I 3 I ~ I ~ 6
htitinl Volume qfliquid (Hl 0) in ini[!JIIgers, (rnl)
I 1oo I 1oo I Silica Gel
Final (g) ___ -1-----4----l-----+-----+----
Initial (g) ___ -1-----4----l-----+----+----
Net (g) ============================~======~======
Total (g)
-... --··---~-------IMPINGERS
Run: Sample Box:
lmpinger Number
_1 -..l..l..LI..i.I...L 6
Initial Volume of liquid ~MzO) In lthpingcl'5, (ml)
'drop out Silica Gel
.I
Final (g) ___ -1-----4----l-----+----~1----
~ti~OO
Net (g):::::::::::::::::::::~:::::::~:::::::.::::::
Total (g)
~
Plant f:.~ ,e.,....,1 LecationL-_5_'{-J. .. _c __________ _
Analytical Method'-------------
>1--r
Average
Net Net
Dale Gas Volume
Test No. 7
Gas Bag No. a--o :!2 l . 8" J.)? (. li--I·&-· /.g-I. g /:;·· Ambient Temp=*=-
Operator
I 7:-1.-I -:;-.z-
Average
Net Net
Volume
Z-o 2·<.'.)
I ~:J..z.._ 11-.Z-
11----T----U·----r----il------'if----ll Average
Ncl Net
Date Gas Volume -----Test No. ____ _
Gas Bag No.-----
Ambient Temp ____ _
Operator ____ _
to2 was determined using a gas analyzer
CO is not measured, as it has the same molecular weight as N2
Yell ow Cake Dryer Baghouse
NYC Baghouse M5
Facility: Energy Fuels Date: 't/ 4./13 __ ___:.....;,;:;. ___ _
Stack Identification: ..:..N;_:Y:....:C=-B=-a:.:J;go;.;h;.;;.ou.;;.;s..:..e ____________ _
IMPINGERS
Xo/OO
IMPINGERS
Final (g)
Initial (g)
Net (g)
Run: Sample Box: f f
lmpioger Number
l I 3 I 4 I -s 6
Initial Volume of liquid (H20) in lmpingCJS, (ml)
l 00 100 I I Silica Gel I
I : • . ~ .
(pft,tt .9 (,Cf(}.l.,. 5" -~~. f e~·f.:t-
lt~'1t . ~~ (p<if).? )?. (,) t'-' ?(iS ·!
-2Z·Cf '·<t S.!> ~~.y
Run: Sample Box:
1m pmger Number
2 I .l.. I 4 I 5 6
Initial Volume of Iiq·uid (1~0) in imJJingers, (m!j
100 100 I I SilicaGel I .
Final (g) -----+----r----+------+-----+----
Initial (g) -----+----1-----+----+----+----
Net (g) ==========================================~
Total (g)
IMPINGERS
IMPINGERS
Run: Sample Box:
lmpinger Number
3 I 4 ! .a. I 6 -I -2
Initial Volume oflirJuld (H,O) in lllpiug..:rs, (ml)
I 00 100 I I Silica Gel I
Final (g) ----~-----~----+-----+-----~-----
Initial (g) _____ --1----t----+----+-----+-----
Net (g) ======================================
Run: Sample Box:
lmpinger .Number
1 . 2 I 3 I 4 I s 6
luilinl Vohtme ofliquid (H20) in imping~rs. (ani)
100· I 00 I I Silica Gel I
Final (g) ___ -if------+----1-----+----+----
Initial (g) -----+----1-----+----+-----+----
Net (g) ========================~============
Total (g)
-------___ ,,
Grizzly Baghouse
IMPINGERS
Filter Number
IMPINGERS
Filter Number
IMPINGERS
Filter Number
Final (g)
Initial (g)
Net (g)
Run:
1
100
'
¥/(or I
~""}.~
-~11. z.
Run:
..L
100
Grizzly
Date: ----------------
----·----
l Sample Box: A
lmpmger Number
2 I ..l.. I 4 I s
lnillnl V'llum~ of liquid (H1Q),in imJiingl:rs, (rnl)
I 00 I I Silica Gel I
' _. . , .
I~ 3 , t Sit.s l1 7o ·4
1oo.o 5 3".0! 'h{.~
l'3·\ s.t... ss .~
2l . '
Sample Box:
lntpingcr Number
..1.. I ..l.. I 4 I i .6
Initial Volume of liquid (Ht-0) in impingers, (m\)
I 00 I I Silica Gel I
Final (g) ------1-----t· ----+----4--------J.-------
Initial (g) ----~---1------1----~------+-----
Net (g) _ ======~====~================~======
Total (g) =======
Sample Box:
I"'p)ngcr Number
1 -:LI..l..l...!.l..a... 6
Initial Volume of liquid (H20) in impingers, (ml)
lOO . 100 I I SilicaGel I
Final (g) ____ +----+-----+-------+----+-----
lnitial (gl ______ +-------l----+----+-----1----
Net (g)=====:!!:::::==d===d===d::=========
Total (g) ==========
Chain of
Custody Record
n\1..4t:U (ICXJ7l -Clitml
Tetco
li#dfil~ · : 391 East 620 South
City American Fork
PrDI«;i Nomft 6:1d l.cUD!Xl (S-1
!~; lz;:~~3
Ener~v Fuels 2013 1st Quarter
Temperature on Receipt---
Drinking Water? Yss 0 No 0
Pro~~
Dean Kitchen
'i"e!C¢'qm ~r i,Arsa r:;t)dti)IF"ax Mlm';Jcr
8014-n-.9106
SMCcnla!:t 1-Lsb Cmci1a
Scott C~ri•t•n•en,GM"ren Palmer
Ci!••iiio\W)'bDI Number
Test America
THE LEADER IN ENVIRONMENTAL TESTING
Da:tt C11Sin ol QJI/cdV NIJIT'br.
4/5/2013
l..ab Nilmbllt' l {-Pagtt of
Analysis (Attach list If
more &Oa09 16 need6d) -:
I I Specla/lnstructJons/ l:ol!ln'r;tiPur<Jn~ Otocrt'C!L-cte_ No. Containers & 0 Conditions ot Rece;pt Matrix Preserv5tives c -... ...
~ '" ::::: ":' -'" N ...,
Sample I. D. No. and Desctfprlon 1 l l ~ ~ ~ ~ ~i ~ ~ 1 ~ .. Date Time ~ ~ s (Ccnta/neiS for eil=h samp~ .my be comblnBd on aneline) I ~ ' I
XlOO Rl Baghouse filter and beaker '4/4/2013 "l 9:00 I X X I -xl I I X098 Rl NYC filters and beaker 4/3/2013 : 7:30 X l
'X099 R2 NYC filters and beaker 4/4/2013 7:30 x l I -I X I I
I I I • l
I I ( I l l i
f .... -· l l I -'--. I I -I j
I I J i
I
l I
PoSsible f'.ll.Uitrl tih(l(lf~C<Jtirm ~~ lf!iiT!~ 0~:14( f4 (A feB may be 8SS«111ed if stiiTI/3fe8l!l'tl mtalned D NOII·Hazstd 0 Fltnlmable 0 Skin lrrit8nt D PoisonS 0 Unlmovm D Fmtum To CJie11t Disposal By Lab 0 Archive For ---Moo/hs iOr>gQf 111an 1 month) ... ~ . ,., -· -e ..... -.. Lo--' ,.....,... ~----~---a-I --· .1 oult· ~~,?'~,. OM-o .. _ I --·---
'· Rt!lW:/uisll/td 1. F/.Qot;.f~ r I OIJf" Ttmll ' c ......,
2. R;J~ . By 2. R.wl';fl!1 By ·-· I !>:Ia 17lmo
3. Rcl"'Jlud.ed By ~~e _ _ 3. RecejY/HJ Eo/
1
~-
1
71m&
C®J/11QI'rl$
When Complete Email to: Dean or Paul [e-mail]
OliiT'RIIJUTION: WnfTF-Re!umedto Ci~ent wrlh Repar~ CA!'IARY-Siiiys Wif!lltle-Samp/9; PINK-Flekl CqJy
...,
&l > 3 g
tr
r & Sl s :J. -~ -fi
Chain of
Custody Record
Temperature on Reeelpt ---
~t24(t007)_ Drinking WatiW? YesD ·NoD
Test America
THE LEADER IN ENVIRONMENTAL TESTING
CAllie! II~~ 1~"-" . Tetro_ l D~-~itclJJ~J:\___ 1.6LoZL2013.
/!ddrl1$B j ~ffl!:rJ!f!!f~~41f.l!!I!TE!ff. -I L!:bNI.W.ilc.' 391 East 620 South __ 1801-492-9106 .• ·_ -
~ I . Zi> C«Jq ~ Ca:mi::t Lim CCntaiCf Aria!ysjs (Attu;h fist tr Amencan_Fork S4_()03 __ -_ ~C~w~mnoo.,....,._,.,.., , fi'IOfe:;p.;;c$tsmsd6d}
~::~~~nd .Quarter l CamerNiaybilNumbar
~~Na. Containers&
Matrix Pmservalives
Sample /.D. No. and Description
• (C<mta/n9tS fortladr sample may bs combined oo ontt liM}
~1 Grizzly filter IX132) and beaker I 6/5,6]13 j[15:00 J~ X! I I I I I I I I I ] I X bdJ lJ
~========---~1! -J,---\ ___ ) I I I I I I I I I I • I II
l_~ ; ~~0~~-:c I --~\.l:S~
~ ~ 1'\ ~\~ llr '·--
~ ,1[-I
-~c=J
L__ ~Ill~ 111\llllllll \111111111 F -.s 120435
-l__],
-.. -. -
0 2Hf~ 0 48Hour.J 0 TDfzy9 0 74~ 0 21 Days 0 an...-.las.oer-rneth~-1
7. ----
Clis:U> of.~ /'J~Jtm>cr
Pegs of t
Speciia/ lnstructionSf
Conditions of Receipt
"<'<\ b ~ ~\.:r"
--\"A-LL c::: z
3. ~""By jee.'v j i1mct la~Gi:Cno:f$)' j D:ml--~nna
~ i When Co~plete Email to: D~an ~r Paul [e-mail]
ii/Sff!JBlJ'tiON! M'IITE'. R&iiiTiciJ u. CJ&ii iilill Riii>Q1i" CWiWi'-~ wlilltfibs.tJi\iiliii Pillk-i'klifC4>f
------------------------------------·----·· -··-.. --··· -·---..
Laboratory Report
Test Dates:
April 3-4, 2013
SDGNo. Order No.
46619
TestAmerlca
rptSTLRchTitle v3.73
TestAmerica
Analytical Data Package Prepared For
Denison Mines (USA) Corp.
Radiochemical Analysis By
TestAmerica
2800 G.W. Way, Richland Wa, 99354, (509)-375-3131.
Assigned Laboratory Code:
Data Package Contains 15 Pages
Report No.: 55334
Results in this report relate only to the sample(s) analyzed.
Client Sample ID (List Order) Lot-811 No. Work Order Report DB ID
X098 R1 NYC filters and J3D100435-2 MOKM21M 9MOKM210
beaker
X099 R2 NYC filters and J301 00435-3 MOKM31AA 9MOKM310
beaker
X100 R1 Baghouse filter J301 00435-1 MOKM11AA 9MOKM110
and be
Page 1 of 15
B11tch No.
3104033
3104033
3104033
Test America
THE LEADER IN ENVIRONMENTAL TESTING
Certificate of Analysis
April30, 2013
Denison Mines (USA) Corp
1050 17th Street, Suite 950
Denver, CO 80265
Attention: Dean Kitchen
Date Received at Lab
Project Name
Sample Type
SDGNumber
I. Introduction
AprillO, 2012
Energy Fuels 2013 1st Quarter
Three (3) Stack Filter Samples
46619
CASE NARRATIVE
On AprillO, 2013, three stack filter samples were received at TestAmerica's Richland laboratory for
radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification
numbers as described on the cover page of the Analytical Data Package report form. The samples were
assigned to Lot Numbers J3Dl00435.
II. Sample Receipt
The samples were received in good condition and no anomalies were noted during check-in.
m. Analytical Results/Methodology
The analytical results for this report are presented by laboratory sample ID. Each set of data includes
sample identification information; analytical results and the appropriate associated statistical
uncertainties.
The analysis requested was:
Alpha Specb·oscopy
Uranium-234, -235, -238 by method RL-ALP-004
IV. Quality Control
The analytical result for each analysis performed includes a minimum of one laboratory control sample
(LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments"
section.
TestAmerica Page 2 of 15
Denison Mines (USA) Corp
April30, 2013
V. Comments
Alpha Spectroscopy
Uranium-234, 235, 238
The LCS, batch blank and sample results are within acceptance limits.
I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically
and for complet-eness, for other than the conditions detailed above. The Laboratory Manager or a
designee, as verified by the following signature has authorized release of the data contained in this hard
copy data package.
Reviewed and approved:
TestAmerica Page 3 of 15
Drinking Water Method Cross References ,..--. ···---~-------. ·--------I ----. --.---
DRINKING WATER ASTM METHOD CROSS REFERENCES ---
Referenced Method lsotope(s) TestAmerica Richland's SOP No.
EPA901.1 Cs-134, 1-131 RL-GAM-001
EPA 900.0 Alpha & Beta Rl -GPC-001
EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002
EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002
EPA 903.1 Ra·226 RL-RA-001
EPA 904.0 Ra-228 RL-RA-001
EPA 905.0 Sr-89/90 RL-GPC-003
ASTM 05174 Uranium RL-KPA-003
EPA 906.0 Tritium RL-LSC·005
I I ! .... f-"· -·----1 .!.' ····-·-:·--·--~ _,,, ·-.. . _.___ -··-
Results in this report relate only to the sample(s) analyzed.
Uncertainty Estimation
TestAmedca Richland has adopted the internationally accepted approach to estimating
m1certainlies described in "NIST Technical Note 1297, 1994 Edition". The approach, "Law of Propagation
of Errors", involves the identification of all variables in an analytical method which are used to derive a
result. These variables are related to the analytical result (R) by some functional relationship, R = constants * f(x,y,z, ... ). Tbe components (x,y,z) are evaluated to determine their contribution to the overall method
uncertainty. The individual component unce1tainties (ui) are then combined using a statistical model that
pro:vides the most probable overall uncertainty value. AU component uncertainties are categorized as type
A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the
components, such as sample homogeneity, are combined with the component uncertainty as the square root
of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result
is the combined uncertainty (uc) multiplied by the coverage factor (1,2, or 3).
When three or more sample replicates are used to derive the analytical result, the type A
uncertainty is the standard deviation of the mean value (S/? n), where S is the standard deviation of the
derived results. The type B uncertainties are all other random or non-random components that are not
included in the standard deviation.
The derivation of the general "Law ofP1·opagation of Errors" equations and specific example are
available on request.
TestAmerlca
rptG~nerallnfo v3.72
TestAmerica Page 4 of 15
--.. .
-----·--
..... --___ ._
, ___
~
• :• . '
' •
Ac[Jun Lev
Batch
Bias
COCNo
C1.1unt Error (lis)
Total Uncert (#s)
u,_Comhlned
Uncertainty.
(#s), Coverugc
Factor
CRDL(RL)
Lc
Lot-Sample No
MDCjMDA
Primary Detector
Ratio U-234/U-238
RsUMDC
RstrrotUcert
Report DB No
RER
SDG
Sum Rpt Alplu
Spec Rst(s)
Work Order
Yield
TestAmerlca
rotGcnernllnfo v3,72
TestAmerica
Report Definitions
An agreed upon activity lovol u~e.d to trigger some action when the finn! n::suh is. greater than or equal to the Action
Level. Often the Action Level is related to the Decision Limit.
The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed
together.
Defined by the equation (Result/Expected)-I as defined by ANSINI3.30.
Chain of Custody Number assigned by tbe Client or TestAmerica.
Poisson counting statistics of the gross sample count and background. The uncertainty is absolute. and in the same
units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background.
AH known uncertainties associated with the preparation and analysis ofthe sample are propagated to give a measure
ofthe uncertainty associated with the result, u. the combined uncertainty. The uncertainty is absolute and In the
same units as the result.
The coverage factor defines the width of the confidence interval, I, 2 or l standard deviations.
Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmerica "default"
nominal detection limit. Often referred to the reporting level (RL)
Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
associated with the sample. The Type I error probability is approximately 5%. Lc=(l.645 •
Sqrt(2*(BkgrndCnt/BkgrndCntMin)/SCntMin)) • (ConvFct/(Eff*Yid*Abn*Vo!) * IngrFct). For LSC methods the
batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count
is zero.
The number assigned by the LIMS software to track samples received on the same day for a given client. The
sample number is a sequential number assigned to each sample in the Lot.
Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
with a Type I and IJ error probability of approximately 5%. MDC = ( 4.65 ~
Sqrt((BkgrndCnt/BkgrndCntMin)/SCntMin) + 2.71/SCntMin) * (ConvFct/(Eff • Yld ~ Abn "'Vol)* IngrFct). For
LSC methods the batch blank is used as a measure of the background variability.
The instrument identifier associated with the analysis of the sample aliquot.
The U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural uranium in NIST SRM 4321C is
1.038.
Ratio of the Result to the MDC. A value greater than 1 may indicate activity above background at a high level of
conftdence. Caution should be used when applying this factor and it should be t1sed in concert with the qualifiers
associated with the result.
Ratio of the Result to the Total Une~;rtainty. If the uncertainty has a coverage factor of 2 a value greater than 1 may
indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence
interval. Caution should be used when applying this factor and it should be used in conce11 with the qualifiers
associated with the result.
Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order
Number.
The equation Replicate Error Ratio~ (S-D}/[sqrt(TPUs2 + TPUd2)] as defined by ICPT BOA where S is the original
sample result, Dis the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the
total uncertainty of the duplicate sample.
Sample Delivery Group Number assigned by the Client or assigned by TcstAmerica upon sample receipt.
The smn of the reported alpha spec results for tests derived from the same sample excluding duplicate result where
the results are in the same units.
The UMS software assign test specific identifier.
The recovery of the tracer added to the sample such as Pu-242 used to trace 11 Pu-239/40 method.
Page 5 of 15
j
Report No. : 55334
Client ld
Batch Work Order Parameter
3104033 FFSR
X098 R1 NYC filters and beaker
MOKM21AA U-234
U-235
U-238
X099 R2 NYC filters and beaker
MOKM31AA U-234
U-235
U-238
X1 00 R1 Baghouse filter and be
MOKM11AA U-234
U-235
U-238
No. of Results: 9
Sample Results Summary
TestAmerica
Ordered by Method, Batch No., Client Sample I D.
Result +-Uncertainty ( zs) Qual Units
1.17E-02 +-1.9E-03 UCI/SA
4.21E-04 +-1.2E-04 UCI/SA
1.12E-02 +-1.8E-03 UCI/SA
1.09E-02 +-1.8E-03 UCI/SA
4.4BE-04 +-1.2E-04 UCI/SA
1.11E-02 +-1.8E-03 UCI/SA
4.22E-02 +-6.6E-03 UCI/SA
2.05E-03 +-3.9E-04 UCI/SA
4.31 E-02 +-6.8E-03 UCJISA
Date: 30-Apr-13
SDG No: 46619
Tracer
Yield MDL CRDL RER2
92% 5.82E-05 9.00E-15
92% 3.22E-05 9.00E-15
92% 5.87E-05 9.00E-15
99% 4.45E-05 9.00E-15
99% 3.72E-05 9.DOE-15
99% 5.16E-05 9.00E·15
92% 4.42E-05 9.00E-15
92% 2.33E-05 9.00E-15
92% 3.28E-05 9.00E-15
TestAmerlca
rptSTLRchSaSum
mary2 V5.2.23
Rl!:llt -R~111lc~te Error Ratio= (S.D)/(sqrt(sq(fi'Us)+sq(TPUd))) ;u defined by ICPT BOA.
• A2002
TestAmerica Page 6 of 15
Report No. : 55334
Batch
Work Order Parameter
FFSR
3104033 BLANK QC,
MOLDR1AA U-234
U-235
U-238
3104033 LCS,
MOLDR1AC U-234
U-238
No. of Results: 5
QC Results Summary
TestAmerica
Ordered by Method, Batch No, QC Type,.
Result+-Uncertainty ( ls) Qual Units
2.37E-08 +-2.8E-08 u UCI/SA
-4.89E-10 +-1.2E-08 u UCI/SA
5.01 E-08 +-3.9E-08 UCI/SA
9.06E-07 +-3.3E-07 UCI/SA
9.23E-07 +-3.3E-07 UCIISA
TestAmerlca Bins • (Result/Expec;ted)-1 as deli ned by ANSI N13.30.
Data: 30-Apr-13
SDG No.: 46619
Tracer lCS
Yield Recovery Bias MDL
93% 4.66E-OB
93% 2.46E-OB
93% 4.19E-OB
93% 93% -0.1 2.90E-08
93% 91% -0.1 3.11E-08
rptSTLRchQcSum U Qunl-Analy:ud (or but not deteded above limiting c•·ltcria, Limit criteria is less thnn the Mdt/Mda/Mdl, Total Unccrt, CRDL, RDL Ol'
mary V5.2.23 not ldcntilietl by gammn scan sortwnrc.
A2002
TestAmerica Page 7 of 15
;nl "' );
3 ~ ('i"
II)
"U II) co m
0> a
~ 01
Lab Name: TestAmerica
Lot-Sample No.: J30100435-2
FORM I
SAMPLE RESULTS
SDG: 46619
Report No. : 55334
Client Sample ID: X098 R1 NYC filters and beaker COCNo.:
Result Count Total MDL, Rpt Unit, Yield Rst/MDL,
P:arameter Qnal En-or ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst!TotUcert
Batch: 3104033 FFSR Work Order: MOKM21AA Report DB 10: 9MOKM21 0
U-234 1.17E-02 S.OE-04 1.9E-03 5.82E-05 UCI/SA 92% (201.5)
2.17E-05 9.00E-15 (12.4)
U-235 4.21E-04 9.6E-05 1.2E-04 3.22E-05 UCI/SA 92% (13.1)
~.75E-06 9.00E-15 (7.3)
U-238 1.12E-02 4.9E-04 1.8E-03 5.87E-05 UCI/SA 92% (190.)
2.20E-05 9.00E-15 (12.4)
Ratio U-234/238 = 1.1
No. of Results: 3 Comments:
Date: 30-Apr-13
Collection Date: 4/3/2013 7:30:00 AM
Received Date: 4/10/2013 1 0:30:00 AM
Matrix: FILTER
Ordered by Client Sample I D. Batch No.
Analysis,
Prep Date
4/25/13 1 0:22 p
4/25/13 10:22 p
4/25/13 1 0:22 p
Total Sa
S"lZe
1.0
Sample
to
Sample
1.0
Sample
Aliquot
Size
0.00119
Sample
0.00119
Sample
0.00119
Sample
Primary
Detector
ALP3
ALP3
ALP3
TestAmerica MDCJMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/McfalMdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
V5.2.23 A2002
~ (/) );
3 ~ ()'
"'
-u "' co m
(0
~
~
01
Lab Name: TestAmerica
Lot-Sample No.: J3D100435-3
Client Sample ID: X099 R2 NYC filters and beaker
Result
Parameter
Count
Qual Error ( 2 s)
Total
Unc:ert(2 s)
FORM I
SAMPLE RESULTS
SDG: 46619
Report No. : 55334
COC No.:
MDL, Rpt Unit, Yield Rst!MDL,
Action Lev Lc: CRDL(RLJ Rst/TotUcert
Batch: 3104033 FFSR Work Order: MOKM31AA Report DB 10: SMOKM31 0
U-234 1.09E.02 4.8E-Q4 1.8E-03 4.45E-05 UCI/SA 99% (245.2)
1.51E-05 9.00E-15 (12.5)
U-235 4.4BE-CU 9.8E-05 1.2E-04 3.72E-05 UCI/SA 99% (12-)
1.15E-05 9.00E-15 (7.5)
U-238 1.11E-02 4,8E-04 1.8E-03 5.16E-05 UCIISA 99% (214.8)
1.87E-05 9.00E-15 (12.5)
Ratio U-2341238 = 1.0
No. of Results: 3 Comments:
·····
Date: 30-Apr-13
Collection Date: 4/4/2013 7:30:00 AM
Received Date: 4/10/2013 10:30:00 AM
Matrix: FILTER
Ordered by Client Sample I D. Batch No.
Anlll:ysis,
Prep Date
4/25/1310:22 p
4/25/13 10:22 p
4/25/13 10:22 p
Total Sa
Size
1.0
Sample
1.0
Sample
1.0
Sample
Aliquot
Size
0.00118
Sample
0.00118
Sample
0.00118
Sample
Primary
Detector
ALP4
ALP4
ALP4
TestAmerica MDCJMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not Identified by gamma scan software.
V5.2.23 A2002
;ni
CJ> ~ 3 ~ r;·
Ill
lJ Ill co CD
~
0
8.
~
U1
-.
Lab Name: TestAmerica
Lot-Sample No.: J3D100435-1
Client Sample ID: X1 00 R1 Bag house filter and be
Result
Parameter
Comrt
Qual Error ( 2 s)
Total
Uncert( 2 s)
FORM I
SAMPLE RESULTS
SDG: 46619
Report No. : 55334
COC No.:
MDL, Rpt Unit, Yield RstiMDL,
Action Lev Lc CRDL(RL] Rst/TotUcert
Batch: 3104033 FFSR Work Order: MOKM11AA Report DB ID: 9MOK.M11 0
LJ-234 4.22E·02 9.9E-04 6.6E-03 4.42E-05 UCI/SA 92% (955.)
1.43E-05 9.00E-15 (12.8)
U-235 2.05E-03 2.2E-04 3.9E-04 2.33E-05 UCI/SA 92% (87.9)
3.81E-06 9.00E-15 (10.6)
U-238 4.31E-02 1.0E-03 6.8E-03 3.28E-05 UCI/SA 92% (1316.2)
8.53E-06 9.00E-15 (12.8)
Ratio U-2341238 = 1.0
No. of Results: 3 Comments:
.....
Date: 30-Apr-13
Collection Date: 4/4/2013 9:00:00 AM
Received Date: 4/10/2013 10:30:00 AM
Matrix: FILTER
Ordered by Client Sample 10, Batch No.
Analysis,
Prep Date
4/25/13 10:21 p
4/25/13 1 0:21 p
4/25/13 1 0:21 p
Total Sa
Size
1.0
Sample
1.0
Sample
1.0
Sample
Aliquot
Size
0.00109
Sample
0.00109
Sample
0.00109
Sample
Primary
Detector
ALP2
ALP2
ALP2
TestAmerica MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSample U Qual-Analyz9d for but not detect9d above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
V5.2..2.3A2002
----------------------------------------------------------.. ·· -···-··..,·--------=-·~=~~--==-----------
--! CD (J) s;
3 CD 5·
"'
"U Ill "' CD
~
~
8.
~
01
Lab Name: TestAmerlca
Matrix: FILTER
Parameter Result Qual
Batch: 3104033 FFSR
U-234 2.37E-08 u
U-235 4.89E-10 u
U-238 5.01E-08
No. of Results: 3 Comments:
Count
Error (2 s)
2.8E-08
1.2E-08
3.7E-08
Tolal
Uncert( 2 s)
FORM 11
BLANK RESULTS
MDL, Rpt Unit,
Lc CRDL Yield
Rst/MDL,
Rst/TotUcert
Woi'K Order: MOLDR1M Report DB ID: MOLDR1AB
2.8E-08 4.66E-08 UCI/SA 93% 0.51
1.50E-08 9.00E-15 (1.7}
12E-08 2.46E-08 UCI/SA 93% -0.02
4.02E-09 9.00E-15 -0.08
3.9E-08 4.19E-08 UC!/SA 93% (1 .2)
1.27E-08 9.00E-15 (2.5)
Ratio U-2341238 = 0.5
Date: 30-Apr-13
SDG: 46619
Report No. : 55334
Analysis, Total Sa Aliquot Primary
Prep Date Size Size Detedor
4/2511310:22 p 0.15 0.15 ALPS
Sample Sample
4/2S/13 10:22 p 0.15 0.15 ALPS
Sample Sample
4/25/13 10:22 p 0.15 0.15 ALPS
Sample Sample
TestAinerica MDCJMDA,Lc-Detection, DeCision Level based on Instrument background or blank, adjust!ld by the sample Efficiency, Yield, and Volume.
rptSTLRchBiank
V5.2.23 A2002
U Qual-Analyzed for l!ut not detected above limiting criteria. Limit criter-ia is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
-~-------···--·-· -~ . -~ ····-·· --·-· ·-------~
col rn l> 3 ~ c;·
D>
"0 D> cc CD
~
1\)
8,
01
Lab Name: TestAmerica
Matrix: FILTER
)lesult Count
Parameter Qual Error ( 2 s)
Total
Uncert(2 5) MDL
FORM II
LCS RESULTS
SDG: 46619
Report No. : 55334
Expected Recovery, Report
Unit Yield E>::pected Uncert Bias
Analysis,
Peep Date
Batch: 3104033
U-234
FFSR Work Order: MOLDR1AC Report DB ID: MOLDR1CS
9.06E-07 1.5E-07 3.3E-07
U-238 9.23E-07 1.5E-07 3.3E-07
No. of Results: 2 Commentsl
TestAmerlca
rptSTL.RchLcs
V5.2.23 A2002
Bias -(Result/E:r:pected)-1 as defined by ANSI N13.30.
2.90E-08 UCI/SA
3.11 E-08 UCI/SA
93% 9.73E-07 5.08E-09 93%
RecLimlts: 70 130 -0.1
93% 1.02E-06 5.32E-09 91%
Rec Limit5: 70 130 -0.1
----------·~--~-----~-------~,~-~~---.-----· --
4/25113 1 0:22 p
4/25/13 1 0:22 p
Date: 30-Apr-13
Allqnot
Size
0.12
Sample
0.12
Sample
Primary
Detector
ALP6
ALP6
;ol (/J );
3 !ll c;·
"'
"0 "' tO ro
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8,
~
01
Chain of
Custody Record
~tZ4(torm
~
Temperatur9 on R9C8ipt ---
Drinking Water? Yes 0 No 0
-~ fFroJeot Msnaper
Tefto 11 Dean Kitchen
-Aildt~· . , ~--~ -~--- -. 13~~ East 620 south \l{8/fll]/lon9~r~eoasllf'il<iNviiiicf ---,_8Q1.:492~9106
Test America
THE LEADER IN ENVIRONMENTAL TESTING
DiJUJ 'I· I 14/512013
l.t!iJ Nu:nl>l:l-
Analysis (/Ut;JCII li$ it
mors spaasl61161!ided) Q1J1 ! ·----:1:~--lstd::cr;m::t jLao COillaa American Fork · : :..._ ~.@_3 1 t s<Oitcorfst .................. .,. '
PrDiol:t N.ome lltlcfLJx.u'otJIS~ CameriWsybfll Nv<~lbsr I j I
a.il~Jcl~~ r . . !
Pllge ( uf t-
Ene Fuels 2013 lst Quarter i I (
~112~/QNo. • ContJJineiS & Ji 0
M8trJX Pre36rV8tives "' "'I"'
5pecJaJ lnstructlon81
Conditions of Receipt
Sampwi.D.No.slldDsSClfprlo/l I Date '~ ~),3 j
(Conlalnets tot sach s=pl• may~ r:omblll~lf an """line) t
Xl~ B~ghous~ filter ~nd beake-;: I I I I I m 'D'( (Y'\ \ :; .. f )(098 I'll NYcfllter$and beaker I I tfY\ONY\ J-..
fwg R2 . NYCfilters.andbeake-r ---,T4/~/20B-~ 7:30 ifXll I I 1 I I r I I I I lxJfl l_f] I I I I I I -' I lY'\0¥...~~
I I -ITT-I I I I I I I I 1 1 ~~o\G::> '-AbS
I I ''''"''I
~_1:5 , ~~~ '~
\'\~ S-<?.-'!:::> . I I I I I
-llllll~llllllll llllllllllllll -. J3 100435
.
-
ldi>nlif.w&m
0 Noii.Hta8Jd 0 Flllfl1mlli>ls D SO:tl/rrilll&1t
·~ liltJCBill rA (A fee msyt» ~if Mmp(~ MJ rei>JintJd 0 Poison B · 0 Unknown I D R"tum To Client N D/spo&31 SyLBb 0 An=hi,.. RJr ___ /IIDnfhs lalg9r ~han 1 m(!llt/2)
11il~d'T7ms~«J
t::;l 24 Hcl,a$ /.JJ ~ ~ 0 T D.liY$ 0 14 Days 0 27 ~ 0 G\'h,:as.Per.meth!Xl J ~~11~-t"S'~ A
I. rJ_, (J.__, J~1klr3 l lth!iit~ ·r;~~~t.~~ ~ ~ -tiilii ~ 14-tD-6 I 10~
~ aey Ia..---,--!fi'liii \a~~ G . lo.;:e IT~nw
a Br lo.rw _ _[~---.. \a-~£1¥ -----~~ -]~ .. I ••
eo-~
When Complete Email to: Dean or Paul [e-mail]
m91Jt!BuTJoNi WHITE -lie!u-d to Cl.liitit ..ntl ~r: CANARY-SlaY$ with tilt> Siiimple; ft'JK • Fi6Ji1 COpy
-----------··-·-
Test America
THE LEADER IN f:!.NVIRONME<.NTAL "I'I:GTING
Sample Check~in List
H:)';)l:J. Container GM Screen Result: (Airlock) ..,..--.:...___:;~--lnilinlsr~] Dateffime Received: ~-~4
Sample GM Screen Result (Sample Receiving) ~--1niti~-]
SDG I~: l\y\..o\0.. NA[] SAF #: _______ N.A ~ Client:~.;.0=-------
Chain of Custody# ________ -------
Shipping Container ID: ___________ N~ Air Bill Number: NA~
Yes~ ] Continue with 1 through 4. Initial appropriate response. Samples received inside shipping container/cooler/box
No [ ] Go to 5, add comment to #16.
1. Custody Seals on shipping container intact? Yes [ No [ No Custody Seal ~ ]
Yes [ No [ No Custody Seal\) ]
___ °C NA~ ]
NA[ Wet[ ] Dry~
2. Custody Seals dated and signed?
3. Cooler temperature:
4. Vermiculite/packing materials is
Item 5 through 16 for samples. Initial appropriate response.
5. Chain of Custody record present? Yctlf ] No [
6. Number of samples received (Each sample may contain multiple bottles):__..J..... _____________ _
7. Containers received: ~~L '.J).(L' 1 S '1\ D~""""'cu:...----------------
8.
9.
10.
11.
Sample holding times exceeded?
Samples have:
___ tape
___ custody seals
'x:
A (FLT, Wipe, Solid, Soil)
S (Air, Niosh 7400)
~~pl::~ in good condition _f-__ are broken
NA[ Yes [ No[~]
~hazard labels f-appropriate sample labels
__ !(Water)
__ T (Biological, Ni-63)
__ are leaking
-~_have air bubbles (Only for samples requiring no head space) Ofuer __________________________________________________ __
12. Sample pi-I appropriate for analysis requested Yes [ ] No [ ] NA lb.. ]
(If acidification is neceswy, then document sample ID, initial pH, amount ofHN03 ndded ~pH afh:r addition on table overleaf)
RPL ID #of preservative used : . ....z..::~l-""-------------------------------
13. Were any anomalies identified in sample receipt? Yes [ ] No ~ ]
Description of anomalies (include sample numbers): NA ,. ____________________ _ 14.
LS-023, Rev. 15,07/11 See over for additional information.
TestAmerica Page 14 of 15
Test America
THE LS:ADER IN E."WIRONMENTAL.. TESTING
15. Sample Location, Sample Collector Listed on COC? *
*For documentation only. No corrective action needed.
Yes [ ] No~ J
16. Additional Tntonnntitm:_Q_I_~-"'~---------------------------
[ ] ClimVCouri<>< d~ture chocl<.
Sample Custodian: ~ 0 ·-~
] Cticnt'/Cowicr unpack cooler.
Dote: L.\-\0...-\ ~
Client Inf01med on. ________ by _________ Person contacted. ________ _
Q(l No action necessary; process as is
ProjectMnnagar ~ ~ Q~ ___ Dnle Lf-10-:0
SAMPLEID Initial pH Acid Amt Final pH SAMPLEID Initial pH AcidAmt Final pH
'\ 1\
""'
\
\ '\
\ "'\
\ ~
\ ~
\ \
\ A \
/~ \ ,1\
L-!L . ~!J
~ ()VJ~,
\· '"' \! ~ 1\G-
s:--. '~--~~
\ . ~~)
\ '\
~ \
\ \
\ \
\ 1\ ~ .
\ '
\
LS-023,Rev.l5,07/ll See over for additional information.
TestAmerica Page 15 of 15
Laboratory Report
Test Dates:
April3-4, 2013
(Samples Re-analyzed for Th-230, Pb-210, and Ra-226)
SDGNo. Order No.
46700
TestAmerica
rptSTLRchTitle v3.73
TestAmerica Laboratories, Inc.
Analytical Data Package Prepared For
Denison Mines (USA) Corp.
Energy Fuels 2013 1st Quarter
Radiochemical Analysis By
TestAmerica
2800 G. W. Way, Richland Wa, 99354, (509)-375-3131.
Assigned Laboratory Code:
Data Package Contains 14 Pages
Report No.: 56105
Results in this report relate only to the sample(s) analyzed.
Client Sample ID (List Order) Lot-Sa No. Work Order Report DB ID
X098 R1 NYC filters and J3E020428-1 MOQQV1AC 9MOQQV10
beaker
X098 R1 NYC filters and J3E020428-1 MOQQV1AA 9MOQQV10
beaker
X098 R1 NYC filters and J3E020428-1 MOQQV1AD 9MOQQV10
beaker
X099 R2 NYC filters and J3E020428-2 MOQQ21AC 9MOQQ210
beaker
X099 R2 NYC filters and J3E020428-2 MOQQ21AA 9MOQQ210
beaker
X099 R2 NYC filters and J3E020428-2 MOQQ21AD 9MOQQ210
beaker
Batch No.
3122080
3122081
3122082
3122080
3122081
3122082
Test America
THE LEADER IN ENVIRONMENTAL TESTING
Certificate of Analysis
July II, 20I3
Denison Mines (USA) Corp
I 050 17th Street, Suite 950
Denver, CO 80265
Attention: Dean Kitchen
Date Received at Lab
Project Name
Sample Type
SDGNumber
I. Introduction
April IO, 2012 I May 2, 2013 (Additional Testing Requested)
Energy Fuels 20 I3 I st Quarter
Two (2) Stack Filter Samples
46700
CASE NARRATIVE
On April IO, 20I3, three stack filter samples were received at TestAmerica's Richland laboratory for
radiochemical analysis. On May 2, 2013, the client requested additional testing for two of the three
samples. Upon receipt, the samples were assigned the TestAmerica identification numbers as described
on the cover page of the Analytical Data Package report form. The samples were re-assigned to Lot
Number J3E020428.
II. Sample Receipt
The samples were received in good condition and no anomalies were noted during check-in.
III. Analytical Results/Methodology
The analytical results for this report are presented by laboratory sample ID. Each set of data includes
sample identification information; analytical results and the appropriate associated statistical
uncertainties.
The analysis requested was:
TestAmerica Laboratories, Inc.
Alpha Spectroscopy
Thorium-228, -230, -232 by method RL-ALP-OOI
Gas Proportional Counting
Pb-2IO by method RL-ALP-Oli
Alpha Scintillation
Radium-226 by method RL-RA-OOI
2
Denison Mines (USA) Corp
July 11, 2013
IV. Quality Control
The analytical result for each analysis performed includes a minimum of one laboratory control sample
(LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments"
section.
V. Comments
Alpha Spectroscopy
Thorium-228, 230, 232
The blank result ofTh-230 has a result above the achieved MDA; suspect some tailing from the Th-229
tracer. The FWHM is elevated, due to the typical and expected tailing from the Th-229 tracer. The
achieved MDA of the samples exceeds the detection limit due insufficient sample volume. There is no
sample volume remaining for re-analysis. Data is reported. Except as noted, the LCS, batch blank and
sample results are within acceptance limits.
Gas Proportional Counting
Pb-210
The achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to
historical process knowledge. The sample activities exceed the MDAs. Data is accepted. Except as
noted, the LCS, batch blank and sample results are within acceptance limits.
Alpha Scintillation
Radium-226
The achieved MDA of the samples exceeds the detection limit due insufficient sample volume. There is
no sample volume remaining for re-analysis. Data is reported. Except as noted, the LCS, batch blank and
sample results are within acceptance limits.
I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically
and for completeness, for other than the conditions detailed above. The Laboratory Manager or a
designee, as verified by the following signature has authorized release of the data contained in this hard
copy data package.
Reviewed and approved:
Erika Jordan
Customer Service Manager
TestAmerica Laboratories, Inc. 3
Drinking Water Method Cross References
DRINKING WATER ASTM METHOD CROSS REFERENCES
Referenced Method lsotope(s) TestAmerica Richland's SOP N
EPA 901 .1 Cs-134, 1-131 RL-GAM-001
EPA 900.0 Alpha & Beta RL-GPC-001
EPA 00-02 Gross Alpha (Coprecipttatjon) RL-GPC-002
EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002
EPA 903.1 Ra-226 RL-RA-001
EPA 904.0 Ra-228 RL-RA-001
EPA 905.0 Sr-89/90 RL-GPC-003
ASTM D5174 Uranium RL-KPA-003
EPA 906.0 Tritium RL-LSC-005
Results in this report relate only to the sample(s) analyzed.
Uncertainty Estimation
TestAmerica Richland has adopted the internationally accepted approach to estimating
uncertainties described in "NIST Technical Note 1297, 1994 Edition". The approach, "Law ofPropagation
of Errors", involves the identification of all variables in an analytical method which are used to derive a
result. These variables are related to the analytical result (R) by some functional relationship, R = constants
* f(x,y,z, ... ). The components (x,y,z) are evaluated to determine their contribution to the overall method
uncertainty. The individual component uncertainties (u;) are then combined using a statistical model that
provides the most probable overall uncertainty value. All component uncertainties are categorized as type
A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the
components, such as sample homogeneity, are combined with the component uncertainty as the square root
of the sum-of-the-squares ofthe individual uncertainties. The uncertainty associated with the derived result
is the combined uncertainty (uc) multiplied by the coverage factor (1 ,2, or 3).
When three or more sample replicates are used to derive the analytical result, the type A
uncertainty is the standard deviation of the mean value (S/?n), where Sis the standard deviation of the
derived results. The type B uncertainties are all other random or non-random components that are not
included in the standard deviation.
The derivation of the general "Law of Propagation of Errors" equations and specific example are
available on request.
TestAmerlca
rptGenerallnfo v3. 72
TestAmerica Laboratories, Inc. 4
o.
Action Lev
Batch
Bias
COCNo
Count Error (#s)
Total Uncert (#s)
Uc_Combined
Uncertainty.
(#s), Coverage
Factor
CRDL (RL)
Lc
Lot-Sample No
MDCI MDA
Primary Detector
Ratio U-234/U-238
Rst/MDC
RstffotUcert
Report DB No
RER
SDG
Sum Rpt Alpha
Spec Rst(s)
Work Order
Yield
TestAmerlca
rptGenerallnfo v3. 72
TestAmerica Laboratories, Inc.
Report Definitions
An agreed upon activity level used to trigger some action when the final result is greater than or equal to the Action
Level. Often the Action Level is related to the Decision Limit.
The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed
together.
Defined by the equation (Result/Expected)-! as defined by ANSI N13.30.
Chain of Custody Number assigned by the Client or TestAmerica.
Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same
units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background.
All known uncertainties associated with the preparation and analysis of the sample are propagated to give a measure
of the uncertainty associated with the result, Uc the combined uncertainty. The uncertainty is absolute and in the
same units as the result.
The coverage factor defines the width of the confidence interval, 1, 2 or 3 standard deviations.
Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmerica "default"
nominal detection limit. Often referred to the reporting level (RL)
Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
associated with the sample. The Type I error probability is approximately 5%. Lc=(l.645 *
Sqrt(2*(BkgrndCnt/BkgrndCntMin)/SCntMin)) * (ConvFct/(Eff*Yld*Abn*Vol) * lngrFct). For LSC methods the
batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count
is zero.
The number assigned by the LIMS software to track samples received on the same day for a given client. The
sample number is a sequential number assigned to each sample in the Lot.
Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
with a Type I and II error probability of approximately 5%. MDC= (4.65 *
Sqrt((BkgmdCnt/BkgrndCntMin)/SCntMin) + 2.71/SCntMin) * (ConvFct/(Etf* Yld * Abn *Vol)* IngrFct). For
LSC methods the batch blank is used as a measure of the background variability.
The instrument identifier associated with the analysis of the sample aliquot.
The U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural uranium in NIST SRM 4321C is
1.038.
Ratio of the Result to the MDC. A value greater than 1 may indicate activity above background at a high level of
confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers
associated with the result.
Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of2 a value greater than I may
indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence
interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers
associated with the result.
San1ple Identifier used by the report system. The number is based upon the first five digits of the Work Order
Number.
The equation Replicate Error Ratio= (S-D)/[sqrt(TPUs2 + TPUd2)] as defined by ICPT BOA where S is the original
sample result, Dis the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the
total uncertainty of the duplicate sample.
Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt.
The sum of the rep01ted alpha spec results for tests derived from the same sample excluding duplicate result where
the results are in the same units.
The LIMS software assign test specific identifier,
The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method.
5
Sample Results Summary Date: 11-Jul-13
TestAmerica
Ordered by Method, Batch No., Client Sample ID.
Report No.: 56105 SDG No: 46700
Client ld Tracer
Batch Work Order Parameter Result+-Uncertainty ( 2s) Qual Units Yield MDL CRDL RER2
3122081 RICHRC5011
X098 R1 NYC filters and beaker
MOQQV1AA TH-228 -4.89E-09 +-8.0E-09 u uCi/Sample 63% 2.85E-08
TH-230 6.35E-07 +-1.2E-07 uCi/Sample 63% 2.15E-08 3.00E-15
TH-232 1.15E-08 +-1.1 E-08 u uCi/Sample 63% 1.41 E-08
X099 R2 NYC filters and beaker
MOQQ21AA TH-228 1.30E-08 +-1.3E-08 u uCi/Sample 49% 1.71 E-08
TH-230 6.65E-07 +-1.3E-07 uCi/Sample 49% 1.30E-08 3.00E-15
TH-232 9.64E-09 +-1.1 E-08 u uCi/Sample 49% 1.58E-08
3122082 RICHRC5011
X098 R1 NYC filters and beaker
MOQQV1AD Pb-210 2.85E-06 +-7.1 E-07 uCi/Sample 49% 6.79E-07 6.00E-14
X099 R2 NYC filters and beaker
MOQQ21AD Pb-210 3.10E-06 +-9.5E-07 uCi/Sample 36% 1.16E-06 6.00E-14
3122080 RL-RA-001
X098 R1 NYC filters and beaker
MOQQV1AC RA-226 8.51 E-08 +-1.9E-07 u uCi/sample 56% 3.81 E-07 9.00E-14
X099 R2 NYC filters and beaker
MOQQ21AC RA-226 -4.46E-08 +-1.9E-07 u uCi/sample 34% 4.35E-07 9.00E-14
. No. of Results: 10
TestAmerica RER2 -Replicate Error Ratio= (S-D)/[sqrt(sq(TPUs)+sq(TPUd))] as defined by ICPT BOA.
rptSTLRchSaSum
mary2 V5.2.23
A2002
U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or
not identified by gamma scan software.
TestAmerica Laboratories, Inc. 6
QC Results Summary Date: 11-Jul-13
TestAmerica
Ordered by Method, Batch No, QC Type,.
Report No. : 561 05 SDG No.: 46700
Batch Tracer LCS
Work Order Parameter Result+-Uncertainty ( 2s) Qual Units Yield Recovery Bias MDL
RICHRC5011
3122081 BLANK QC,
MOQTJ1AA TH-228 7.53E-10 +-8.6E-09 u uCi/Sample 42% 2.59E-08
TH-230 4.56E-08 +-2.7E-08 uCi/Sample 42% 2.37E-08
TH-232 3.46E-09 +-7.5E-09 u uCi/Sample 42% 1.95E-08
3122081 LCS,
MOQTJ1AC TH-230 2.18E-06 +-3.9E-07 uCi/Sample 34% 97% 0.0 2.17E-08
RICHRC5011
3122082 BLANK QC,
MOQTK1AA Pb-210 1.95E-07 +-2.4E-07 u JCi/Sample 82% 3.85E-07
3122082 LCS,
MOQTK1AC PB-210 1,01 E-05 +-1.8E-06 uCi/Sample 82% 111% 0.1 4.10E-07
RL-RA-001
3122080 BLANK QC,
MOQTH1AA RA-226 3.88E-09 +-8.5E-08 u uCi/sample 94% 1.80E-07
3122080 LCS,
MOQTH1AC RA-226 1.24E-05 +-3.3E-06 uCi/sample 94% 125% 0.3 2.31E-07
No. of Results: 8
TestAmerica Bias -(Result/Expected)-I as defined by ANSI N13.30.
rptSTLRchQcSum U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or
mary V5.2.23 not identified by gamma scan software.
A2002
TestAmerica Laboratories, Inc. 7
FORM I Date: 11-Jul-13
SAMPLE RESULTS
Lab Name: TestAmerica SDG: 46700 Collection Date: 4/3/2013 7:30:00 AM
Lot-Sample No.: J3E020428-1 Report No.: 56105 Received Date: 5/2/2013 12:05:00 PM
Client Sample ID: X098 R1 NYC filters and beaker COC No.: Matrix: FILTER
Ener~~ Fuels 2013 1st Quarter Ordered by Client Sample ID, Batch No.
Result Count Total MDL, Rpt Unit, Yield Rst/MDL, Analysis, Total Sa Aliquot Primary
Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Prep Date Size Size Detector
Batch: 3122080 RL-RA-001 Work Order: MOQQV1AC Report DB ID: 9MOQQV10
RA-226 8.51 E-08 u 1.9E-07 1.9E-07 3.81 E-07 uCi/sample 56% 0.22 7/2/13 07:13 p 1.0 0,9821 ASCEHA
1.72E-07 9.00E-14 0.87 Sample Sample
Batch: 3122081 RICHRC5011 Work Order: MOQQV1AA Report DB ID: 9MOQQV10
TH-228 -4.89E-09 U 7.9E-09 8.0E-09 2.85E-08 uCi/Sample 63% -0.17 6/28/13 03:50 a 1.0 0.98212 ALP121
1.06E-08 -(1.2) Sample Sample
TH-230 6.35E-07 B.OE-08 1.2E-07 2.15E-08 uCi/Sample 63% (29.6) 6/28/13 03:50 a 1.0 0.98212 ALP121
7.35E-09 3.00E-15 (10.2) Sample Sample
TH-232 1.15E-08 u 1.1 E-08 1.1 E-08 1.41 E-08 uCi/Sample 63% 0.81 6/28/13 03:50 a 1.0 0.98212 ALP121
3.67E-09 (2.) Sample Sample
Batch: 3122082 RICHRC5011 Work Order: MOQQV1AD Report DB ID: 9MOQQV10
Pb-210 2.85E-06 5.0E-07 7.1 E-07 6.79E-07 uCi/Sample 49% (4.2) 7/5/1311:19 a 1.0 0.98212 GPC32C
329E-07 6.00E-14 (8.) Sample Sample
No. of Results: 5 Comments:
TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSample U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
V5.2.23 A2002
TestAmerica Laboratories, Inc. 8
FORM I Date: 11-Jul-13
SAMPLE RESULTS
Lab Name: TestAmerica SDG: 46700 Collection Date: 4/4/2013 7:30:00 AM
Lot-Sample No.: J3E020428-2 Report No.: 56105 Received Date: 5/2/2013 12:05:00 PM
Client Sample ID: X099 R2 NYC filters and beaker COC No.: Matrix: FILTER
Ener~~ Fuels 2013 1st Quarter Ordered b~ Client SamEie ID, Batch No.
Result Count Total MDL, Rpt Unit, Yield Rst/MDL, Analysis, Total Sa Aliquot Primary
Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Prep Date Size Size Detector
Batch: 3122080 RL-RA-001 Work Order: MOQQ21AC Report DB ID: 9MOQQ210
RA-226 -4.46E-08 U 1,9E-07 1.9E-07 4.35E-07 uCi/sample 34% -0,1 7/2/13 07:13 p 1.0 0.9756 ASCGAB
1.87E-07 9.00E-14 -0.48 Sample Sample
Batch: 3122081 RICHRC5011 Work Order: MOQQ21AA Report DB ID: 9MOQQ210
TH-228 1.30E-08 u 1.3E-08 1.3E-08 1. 71 E-08 uCi/Sample 49% 0.76 6/28/13 04:13 a 1.0 0.97558 ALP118
5.19E-09 (2.) Sample Sample
TH-230 6.65E-07 7.8E-08 1.3E-07 1.30E-08 uCi/Sample 49% (51.3) 6/28/13 04:13 a 1.0 0.97558 ALP118
3.38E-09 3.00E-15 (10.5) Sample Sample
TH-232 9.64E-09 u 1.1 E-08 1.1 E-08 1.58E-08 uCi/Sample 49% 0.61 6/28/13 04:13 a 1.0 0.97558 ALP118
4.77E-09 (1.8) Sample Sample
Batch: 3122082 RICHRC5011 Work Order: MOQQ21AD Report DB ID: 9MOQQ210
Pb-210 3.10E-06 7.9E-07 9.5E-07 1.16E-06 uCi/Sample 36% (2. 7) 7/5/13 11 : 19 a 1.0 0.97558 GPC32D
5.63E-07 6.00E-14 (6.5) Sample Sample
No. of Results: 5 Comments:
TestAmerica MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
V5.2.23 A2002
TestAmerica Laboratories, Inc. 9
FORM II Date: 11-Jul-13
BLANK RESULTS
Lab Name: TestAmerica SDG: 46700
Matrix: FILTER Report No.: 56105
Count Total MDL, Rpt Unit, Rst/MDL, Analysis, Total Sa Aliquot Primary
Parameter Result Qual Error ( 2 s) Uncert( 2 s) Lc CRDL Yield Rst!TotUcert Prep Date Size Size Detector
Batch: 3122082 RICHRC5011 Work Order: MOQTK1AA Report DB ID: MOQTK1AB
Pb-210 1.95E-07 u 2.3E-07 2.4E-07 3.85E-07 uCi/Sample 82% 0.51 7/5/13 06:47 p 1.0 1.0 GPC31B
1.86E-07 6,00E-14 (1 .6) Sample Sample
Batch: 3122080 RL-RA-001 Work Order: MOQTH1AA Report DB ID: MOQTH1AB
RA-226 3.88E-09 u 8.5E-08 8,5E-08 1.80E-07 uCilsample 94% 0.02 7/2/13 07:13 p 1.0 1.0 ASCHMA
7.97E-08 9.00E-14 0.09 Sample Sample
Batch: 3122081 RICHRC5011 Work Order: MOQTJ1AA Report DB ID: MOQTJ1AB
TH-228 7.53E-10 u 8.6E-09 8.6E-09 2.59E-08 uCi/Sample 42% 0.03 6/28/13 03:54 a 1.0 1.0 ALP123
7.83E-09 0.17 Sample Sample
TH-230 4.56E-08 2.6E-08 2,7E-08 2.37E-08 uCi/Sample 42% (1.9) 6/28/13 03:54 a 1.0 1.0 ALP123
7, 19E-09 3.00E-15 (3.4) Sample Sample
TH-232 3.46E-09 u 7.4E-09 7.5E-09 1.95E-08 uCi/Sample 42% 0.18 6/28/13 03:54 a 1.0 1.0 ALP123
5.09E-09 0.93 Sample Sample
No. of Results: 5 Comments:
TestAmerica MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchBiank U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
V5.2.23 A2002
TestAmerica Laboratories, Inc. 10
Lab Name: TestAmerica
Matrix: FILTER
Count
Parameter Result Qual Error ( 2 s)
Batch: 3122082 RICHRC5011
PB-210 1.01 E-05 5.0E-07
Batch: 3122080 RL-RA-001
RA-226 1.24E-05 7.5E-07
Batch: 3122081 RICHRC5011
TH-230 2.18E-06 1.8E-07
No. of Results: 3 Comments:
Total
Uncert( 2 s) MDL
FORM II
LCS RESULTS
Report
Unit Yield
Expected
Expected Uncert
Work Order: MOQTK1AC Report DB ID: MOQTK1CS
1.8E-06 4.1 OE-07 uCi/Sample 82% 9.11 E-06 1.53E-07
Rec Limits: 75 125
Work Order: MOQTH1AC Report DB ID: MOQTH1CS
3.3E-06 2.31 E-07 uCi/sample 94% 9.90E-06 1.01 E-07
Rec Limits: 75 125
Work Order: MOOT J1AC Report DB ID: MOQTJ1CS
3.9E-07 2.17E-08 uCi/Sample 34% 2.25E-06 2.33E-08
Rec Limits: 75 125
TestAmerica Bias -(Result/Expected)-I as defined by ANSI N13.30.
rptSTLRchlcs
V5.2.23 A2002
TestAmerica Laboratories, Inc. 11
Date: 11-Jul-13
SDG: 46700
Report No.: 56105
Recovery, Analysis, Aliquot Primary
Bias Prep Date Size Detector
111% 7/5/13 06:47 p 1.0 GPC31C
0.1 Sample
125% 7/3/13 08:30 a 1.0 ASCKMD
0.3 Sample
97% 6/28/13 03:54 a 1.0 ALP124
0.0 Sample
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THE LEADER I~ eNVIAQNMS.NTA.l. TEEmNG
Sample Check-in List
Date/Time Received:_~ t:! .... \ "-\ l~"b.Q Container GM Screen Result: (Airlock) -:-----:"':::---fnlliolsf~] ~ Sample GM Screen Result (Sample Receiving) ~--lniliul~:f)
Client: }::>(:.0 SDG#: l\u\.o\0... NA[] SAF #:.~ ______ N.A~
Lot Number: ~?-:>'\i.>\C:DU..~ S
CbamofCusrody# ________________ -----------------------------------------------------~
Shippmg Container ID:. ____________________ N~ Air Bill Number: NA~
Samples received inside shlppmg container/cooler/box Yes~ ] Continue with 1 through 4, Initial appropriate response.
No [ ] Go to 5, add comment to #16.
1. Custody Seals on shipping container mtact? Yes [ No [ No Custody Seal ~]
Yes [ No [ No Cusrody Seal\') J
___ oc NA~ ]
NA [ Wet [ ] Dry~
2. Custody Seals dated and signed?
3. Cooler temperature:
4. Vermiculite/packmg materials is
Item 5 through 16 for samples, Initial appropriate response.
5. Chain of Custody record present? vJly ] No [
6. Number of samples received (Each sample may contain multiple ~!tles):,__,...~.-_________________________ _
8.
9.
10.
11.
Sample holding times exceeded?
Samples have:
____ tape
__ custody seals
llriX:
A (~ 1 Wipe, Solid, SoU)
S (Alt. Niosh 7400)
NA[ Yes[
~hazard labels
f--appropriate sample labels
__ I(Water)
___ T (Biological, Ni-63)
No[~]
~pi:;~ in good condition are leaking
--?-are broken _ have air bubbles (Only for samples requiring no head space)
_____ ofu~-----------------------------------------------------------------------
12, Sample pH appropriate for analysis requested Yes [ ] No [ ] NA (h. ]
(If acidification is necessary, then document sample ID, initial pH, amount ofHN03 added ~pH aft~:r addition on table overleaf)
RPL ID # of preservative used :._vJ~I..ci'-----------------------------------'----------------
13. Were any anomalies identified in sample receipt? Yes [ ] No~ ]
14. Description of anomalies (include sample numbers): NA '·W------------------------------------
LS-023, Rev. 15, 07/11
TestAmerica
TestAmerica Laboratories, Inc.
Page 14 of 15
13
See over for additional information.
Test America
tHE LEADER IN E.~VIRONMENTAL U:S'TINQ
15. Sample Location, Sample Collector Listed on COC? ,..
*For documentation only. No corrective action11eeded.
Yes [ ] No~]
16. Additional Information:_Q...\...z::-----------------------------
[ ] ClirutliCon>i« don~e.ature oh~k
Sample Custodian: y. o...:..... ~
] Client/Courier unpack cooler.
Date: L\-\0--\~
Client Infmmed on. ________ by _________ Person contacted ________ _
!XJ No action necessary; process as is
ProjectManagcr ~~ QO!~
SAMPLE ID Initial pH Acid Amt Final pH SAMPLEID I Initial pH AcidAmt Final pH
"' \
\ \
\ \
~ '\
\ '\
\ '\
\ \
\ A \
/ ~~ \ .....
l,... ~r \II
~-' _\ . ~ e
'\ ~"'1. \G-
I\' '· \~
\ \{)
~ \
\ \
\ \
\ \
\.
1\ ' \ '
\
LS-023, Rev. 15,07/11 See over for additional information.
TestAmerica
TestAmerica Laboratories, Inc.
Page 15 of 15
14
Laboratory Report
Test Dates:
June 5-6, 2013
SDGNo. Order No.
46884
TestAmerica
rptSTLRchTitle v3. 73
TestAmerica Laboratories, Inc.
Analytical Data Package Prepared For
Denison Mines (USA) Corp.
Denison Mines 2013 2nd Quarter
Radiochemical Analysis By
TestAmerica
2800 G. W. Way, Richland Wa, 99354, (509)-375-3131.
Assigned Laboratory Code:
Data Package Contains 12 Pages
Report No.: 56176
Results in this report relate only to the sample(s) analyzed.
Client Sample ID (List Order) Lot-Sa No. Work Order Report DB ID
R1 Grizzly filter (X132)and J3F120435-1 M04KG1AC 9M04KG10
be
R1 Grizzly filter (X132)and J3F120435-1 M04KG1AA 9M04KG10
be
Batch No.
3172023
3172024
Test America
THE LEADER IN ENVIRONMENTAL TESTING
Certificate of Analysis
July 17,2013
Denison Mines (USA) Corp
1050 17th Street, Suite 950
Denver, CO 80265
Attention: Dean Kitchen
Date Received at Lab
Project Name
Sample Type
SDGNumber
I. Introduction
June 11, 2012
Energy Fuels 2013 2nd Quarter
One (1) Stack Filter Sample
46884
CASE NARRATIVE
On June 11, 2013, one stack filter sample was received at TestAmerica's Richland laboratory for
radiochemical analysis. Upon receipt, the sample was assigned the TestAmerica identification numbers
as described on the cover page of the Analytical Data Package report form. The sample was assigned to
Lot Numbers J3F120435.
II. Sample Receipt
The sample was received in good condition and no anomalies were noted during check-in.
III. Analytical Results/Methodology
The analytical results for this report are presented by laboratory sample ID. Each set of data includes
sample identification information; analytical results and the appropriate associated statistical
uncertainties.
The analysis requested was:
TestAmerica Laboratories, Inc.
Alpha Spectroscopy
Uranium-234, -235, -238 by method RL-ALP-004
Thorium-228, -230, -232 by method RL-ALP-001
2
Denison Mines (USA) Corp
July 17,2013
IV. Quality Control
The analytical result for each analysis performed includes a minimum of one laboratory control sample
(LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments"
section.
V. Comments
Alpha Spectroscopy
Thorium-228, 230, 232
The blank result ofTh-230 has a result above the achieved MDA; suspect some tailing from the Th-229
tracer. The FWHM is elevated, due to the typical and expected tailing from the Th-229 tracer. The
achieved MDA of the samples exceeds the detection limit due insufficient sample volume. There is no
sample volume remaining for re-analysis. Data is reported. Except as noted, the LCS, batch blank and
sample results are within acceptance limits.
Uranium-234, 235. 238
The achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to
historical process knowledge. The sample activities exceed the MDAs. Data is accepted. Except as
noted, the LCS, batch blank and sample results are within acceptance limits.
I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically
and for completeness, for other than the conditions detailed above. The Laboratory Manager or a
designee, as verified by the following signature has authorized release of the data contained in this hard
copy data package.
Reviewed and approved:
Erika Jordan
Customer Service Manager
TestAmerica Laboratories, Inc. 3
Drinking Water Method Cross References
DRINKING WATER ASTM METHOD CROSS REFERENCES
Referenced Method lsotope(s) TestAmerica Richland's SOP N
EPA 901.1 Cs-134, 1-131 RL-GAM-001
EPA 900.0 Alpha & Beta RL-GPC-001
EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002
EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002
EPA 903.1 Ra-226 RL-RA-001
EPA 904.0 Ra-228 RL-RA-001
EPA 905.0 Sr-89/90 RL-GPC-003
ASTM D5174 Uranium RL-KPA-003
EPA 906.0 Tritium RL-LSC-005
Results in this report relate only to the sample(s) analyzed.
Uncertainty Estimation
TestAmerica Richland has adopted the internationally accepted approach to estimating
uncertainties described in "NIST Technical Note 1297, 1994 Edition". The approach, "Law ofPropagation
ofErrors", involves the identification of all variables in an analytical method which are used to derive a
result. These variables are related to the analytical result (R) by some functional relationship, R = constants
* f{x,y,z, ... ). The components (x,y,z) are evaluated to determine their contribution to the overall method
uncertainty. The individual component uncertainties (u;) are then combined using a statistical model that
provides the most probable overall uncertainty value. All component uncertainties are categorized as type
A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the
components, such as sample homogeneity, are combined with the component uncertainty as the square root
of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result
is the combined uncertainty (uc) multiplied by the coverage factor (1 ,2, or 3).
When three or more sample replicates are used to derive the analytical result, the type A
uncertainty is the standard deviation of the mean value (S/?n), where Sis the standard deviation of the
derived results. The type B uncertainties are all other random or non-random components that are not
included in the standard deviation.
0.
The derivation of the general "Law of Propagation ofErrors" equations and specific example are
available on request. --~------------------------------------------------------------
TestAmerica
rptGenerallnfo v3. 72
TestAmerica Laboratories, Inc. 4
Action Lev
Batch
Bias
COCNo
Count Error (#s)
Total Uncert (#s)
Uc-Combined
Uncertainty.
(#s), Coverage
Factor
CRDL (RL)
Lc
Lot-Sample No
MDCI MDA
Primary Detector
Ratio U-234/U-238
Rst/MDC
Rst/TotUcert
Report DB No
RER
SDG
Sum Rpt Alpha
Spec Rst(s)
Work Order
Yield
TestAmerica
rptGenerallnfo v3. 72
TestAmerica Laboratories, Inc.
Report Definitions
An agreed upon activity level used to trigger some action when the final result is greater than or equal to the Action
Level. Often the Action Level is related to the Decision Limit.
The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed
together.
Defined by the equation (Result/Expected)-I as defined by ANSI N13.30.
Chain of Custody Number assigned by the Client or TestAmerica.
Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same
units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background.
All known uncertainties associated with the preparation and analysis of the sample are propagated to give a measure
of the uncertainty associated with the result, Uc the combined uncertainty. The uncertainty is absolute and in the
same units as the result.
The coverage factor defines the width of the confidence interval, 1, 2 or 3 standard deviations.
Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmerica "default"
nominal detection limit. Often referred to the reporting level (RL)
Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
associated with the sample. The Type I error probability is approximately 5%. Lc=(1.645 *
Sqrt(2*(BkgrndCnt/BkgrndCntMin)/SCntMin)) * (ConvFct/(Eff*Yid*Abn*Vol) * IngrFct). For LSC methods the
batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count
is zero.
The number assigned by the LIMS software to track samples received on the same day for a given client. The
sample number is a sequential number assigned to each sample in the Lot.
Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
with a Type I and II error probability of approximately 5%. MDC= (4.65 *
Sqrt((BkgmdCnt/BkgmdCntMin)/SCntMin) + 2.71/SCntMin) * (ConvFct/(Eff * Yld * Abn *Vol)* IngrFct). For
LSC methods the batch blank is used as a measure of the background variability.
The instrument identifier associated with the analysis of the sample aliquot.
The U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural uranium in NIST SRM 4321C is
1.038.
Ratio of the Result to the MDC. A value greater than 1 may indicate activity above background at a high level of
confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers
associated with the result.
Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of2 a value greater than 1 may
indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence
interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers
associated with the result.
Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order
Number.
The equation Replicate Error Ratio= (S-D)/[sqrt(TPUs2 + TPUd2)] as defined by ICPT BOA where S is the original
sample result, D is the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the
total uncertainty of the duplicate sample.
Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt.
The sum of the reported alpha spec results for tests derived from the same sample excluding duplicate result where
the results are in the same units.
The LIMS software assign test specific identifier.
The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method.
5
Report No. : 56176
Client ld
Batch Work Order Parameter
3172024 RICHRC5011
R1 Grizzly filter (X132)and be
M04KG1AA TH-228
TH-230
TH-232
3172023 FFSR
R1 Grizzly filter (X132)and be
M04KG1AC U-234
U-235
U-238
No. of Results: 6
Sample Results Summary
TestAmerica
Ordered by Method, Batch No., Client Sample ID.
Date: 17-Jul-13
SDG No: 46884
Result+-Uncertainty ( 2s)
1.48E-08 +-1.0E-08
1.28E-06 +-2.1 E-07
3.08E-08 +-1.3E-08
5.82E-05 +-4.3E-05
1.47E-05 +-2.1 E-05
5.09E-05 +-4.0E-05
Qual Units
Tracer
Yield
uCi/Sample 93%
uCi/Sample 93%
uCi/Sample 93%
uCi/Sample 77%
U uCi/Sample 77%
uCi/Sample 77%
MDL CRDL
1.38E-08
1.21E-08 3.00E-15
8.39E-09
2,96E-05 9.00E-15
2.96E-05 9.00E-15
2.96E-05 9.00E-15
RER2
TestAmerica RER2 -Replicate Error Ratio= (S-D)/[sqrt(sq(TPUs)+sq(TPUd))] as defined by ICPT BOA.
rptSTLRchSaSum
mary2 V5.2.23
A2002
U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or
not identified by gamma scan software.
TestAmerica Laboratories, Inc. 6
QC Results Summary Date: 17-Jul-13
TestAmerica
Ordered by Method, Batch No, QC Type,.
Report No. : 56176 SDG No.: 46884
Batch Tracer LCS
Work Order Parameter Result+-Uncertainty ( 2s) Qual Units Yield Recovery Bias MDL
RICHRC5011
3172024 BLANK QC,
M06WL1AA TH-228 2.71E-10 +-3, 1E-09 u uCi!Sample 84% 9.31E-09
TH-230 2.51 E-08 +-1.2E-08 JCi/Sample 84% 7.46E-09
TH-232 2.64E-10 +-3.0E-09 u uCi/Sample 84% 9.07E-09
3172024 LCS,
M06WL1AC TH-230 1. 76E-06 +-2. 9E-07 uCi/Sample 96% 97% 0.0 9.14E-09
FFSR
3172023 BLANK QC,
M06WK1AA U-234 1.09E-07 +-1.4E-07 u JCi/Sample 94% 2.18E-07
U-235 7.51 E-08 +-1.2E-07 u uCi/Sample 94% 1.87E-07
U-238 1.16E-07 +-1.4E-07 u uCi/Sample 94% 1.87E-07
3172023 LCS,
M06WK1AC U-234 2.48E-05 +-5.0E-06 uCi/Sample 59% 107% 0.1 3.07E-07
U-238 2.34E-05 +-4. 7E-06 uCi/Sample 59% 97% 0.0 3.07E-07
No. of Results: 9
TestAmerica Bias -(Result/Expected)-1 as defined by ANSI N13.30.
rptSTLRchQcSum U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or
mary V5.2.23 not identified by gamma scan software.
A2002
TestAmerica Laboratories, Inc. 7
FORM I Date: 17-Jul-13
SAMPLE RESULTS
Lab Name: TestAmerica SDG: 46884 Collection Date: 6/5/2013 3:00:00 PM
Lot-Sample No.: J3F120435-1 Report No.: 56176 Received Date: 6/11/2013 12:45:00 PM
Client Sample ID: R1 Grizzly filter (X132)and be COC No.: Matrix: FILTER
Denison Mines 2013 2nd Quarter Ordered by Client Sample I D. Batch No.
Result Count Total MDL, Rpt Unit, Yield Rst/MDL, Analysis, Total Sa Aliquot Primary
Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDL(RL) Rst/TotUcert Prep Date Size Size Detector
Batch: 3172023 FFSR Work Order: M04KG1AC Report DB ID: 9M04KG10
U-234 5.82E-05 4.2E-05 4.3E-05 2.96E-05 uCi/Sample 77% (2.) 7/1/13 10:55 p 1.0 0.00104 ALP219
4.84E-06 9.00E-15 (2.7) Sample Sample
U-235 1.47E-05 u 2.1E-05 2.1 E-05 2.96E-05 uCi/Sample 77% 0.5 7/1/13 10:55 p 1.0 0.00104 ALP219
4.84E-06 9.00E-15 (1.4) Sample Sample
U-238 5.09E-05 3.9E-05 4.0E-05 2.96E-05 uCi/Sample 77% (1. 7) 7/1/13 10:55 p 1.0 0.00104 ALP219
4.84E-06 9.00E-15 (2.6) Sample Sample
Ratio U-2341238 = 1.1
Batch: 3172024 RICHRC5011 Work Order: M04KG1AA Report DB ID: 9M04KG10
TH-228 1.48E-08 1 ,OE-08 1,0E-08 1.38E-08 uCi/Sample 93% (1.1) 7/2/13 09:50 a 1.0 0.98048 ALP117
5.22E-09 (2.9) Sample Sample
TH-230 1.28E-06 7.9E-08 2.1 E-07 1.21 E-08 uCi/Sample 93% (105.6) 7/2/13 09:50 a 1.0 0.98048 ALP117
4.40E-09 3.00E-15 (12.) Sample Sample
TH-232 3.08E-08 1.3E-08 1.3E-08 8.39E-09 uCi/Sample 93% (3. 7) 7/2/13 09:50 a 1.0 0.98048 ALP117
2.54E-09 (4.6) Sample Sample ----~
No. of Results: 6 Comments:
TestAmerica MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
V5.2.23 A2002
TestAmerica Laboratories, Inc. 8
FORM II Date: 17-Jul-13
BLANK RESULTS
Lab Name: TestAmerica SDG: 46884
Matrix: FILTER Report No.: 56176
Count Total MDL, Rpt Unit, Rst/MDL, Analysis, Total Sa Aliquot Primary
Parameter Result Qual Error ( 2 s) Uncert( 2 s) Lc CRDL Yield Rst/TotUcert Prep Date Size Size Detector
Batch: 3172023 FFSR Work Order: M06WK1AA Report DB ID: M06WK1AB
U-234 1.09E-07 u 1.4E-07 1.4E-07 2.18E-07 uCi/Sample 94% 0.5 7/1/1310:55 p 1.0 0.17 ALP220
5.37E-08 9.00E-15 (1 .5) Sample Sample
U-235 7.51E-08 u 1.2E-07 1.2E-07 1.87E-07 uCi/Sample 94% 0.4 7/1/1310:55 p 1.0 0.17 ALP220
3.80E-08 9.00E-15 (1.3) Sample Sample
U-238 1.16E-07 u 1.4E-07 1.4E-07 1.87E-07 uCi/Sample 94% 0.62 7/1/13 10:55 p 1.0 0.17 ALP220
3.80E-08 9.00E-15 (1 .6) Sample Sample
Ratio U-2341238 = 0.9
Batch: 3172024 RICHRC5011 Work Order: M06WL 1AA Report DB ID: M06WL 1AB
TH-228 2.71E-10 u 3.1E-09 3.1 E-09 9.31 E-09 uCi/Sample 84% 0.03 7/2/13 09:51 a 1.0 1.0 ALP118
2.82E-09 0.17 Sample Sample
TH-230 2.51E-08 1.2E-08 1.2E-08 7.46E-09 uCi/Sample 84% (3.4) 7/2/13 09:51 a 1.0 1.0 ALP118
1.94E-09 3.00E-15 (4.1) Sample Sample
TH-232 2.64E-10 u 3.0E-09 3.0E-09 9.07E-09 uCi/Sample 84% 0.03 7/2/13 09:51 a 1.0 1.0 ALP118
2.75E-09 0.17 Sample Sample
No. of Results: 6 Comments:
TestAmerica MDCIMDA,Lc-Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume.
rptSTLRchBiank U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software.
V5.2.23 A2002
TestAmerica Laboratories, Inc. 9
Lab Name: TestAmerica
Matrix: FILTER
Count
Parameter Result Qual Error ( 2 s)
Batch: 3172023 FFSR
U-234 2.48E-05 2.7E-06
U-238 2.34E-05 2.7E-06
Batch: 3172024 RICHRC5011
TH-230 1.76E-06 9.7E-08
No. of Results: 3 Comments:
Total
Uncert( 2 s) MDL
FORM II
LCS RESULTS
Report
Unit Yield
Expected
Expected Uncert
Work Order: M06WK1AC Report DB ID: M06WK1CS
5.0E-06 3.07E-07 uCi/Sample 59% 2.31 E-05 1.22E..Q7
Rec Limits: 75 125
4.7E-06 3.07E-07 uCi/Sample 59% 2.42E-05 1.28E-07
Rec Limits: 75 125
Work Order: M06WL 1AC Report DB ID: M06WL 1 CS
2.9E-07 9.14E-09 uCi/Sample 96% 1.82E-06 1.88E-08
Rec Limits: 75 125
TestAmerica
rptSTLRchlcs
V5.2.23 A2002
Bias -(Result/Expected)-I as defined by ANSI N13.30.
TestAmerica Laboratories, Inc. 10
Date: 17-Jul-13
SDG: 46884
Report No.: 56176
Recovery, Analysis, Aliquot Primary
Bias Prep Date Size Detector
107% 7/1/13 10:56 p 0.14 ALP221
0.1 Sample
97% 7/1/13 10:56 p 0.14 ALP221
0.0 Sample
97% 7/2/13 09:51 a 1.0 ALP119
0.0 Sample
;l :;.
3 co .... c:;·
I>'
1:""' §..
0 ~ .... c;·
·"' S' ~
--
Chain of
Custody Record
'TI\l:.-4124 (111Cl7)
Cf!8ml Tetco
Addtess, 391 East 620 South
Ci<Y I American Fork l ~lZioCodo t. . 84003 ---·
~~"';nd Quarter
~0rti911QurJle(ifp.
Sample 1.0. No. snd Description Date (Ccma!Mrs for each sample may be combined on one Rne)
f Rl Grizzly filter (Xl32) and beaker
-
6/5.6/13
r
I ~~I:\'Aa~C:... -!
j ~~ \ . ...-----\4:~'l; <{"--\ .t -j -r ~ _0 ~ -c\-\..,__ I
I ___ J I
[~ Ill' Ill~ lllllllllllllll\llll\1 Jl -
J3 120435 -
-
I
Temperature on Receipt __ _ Test America
Drinking Water? Yes 0 ·No 0 THE LEADER IN ENVIRONMENTAL TESTING
,~~"~"""""' 1r o~be11 ~ .
I SJJSlli2.o'J. 3-I CJurm of~ Nl/ll'lbQr
_j ~-t:i!f!!!1J5J!J~JtF~ IJJbNumw
. 801-492-9106 ' ,! Fags of
SileC<miaa I I.sb Contac! Analysis (Attach list If l _I Scutt auistensen, GarTen Palmer more space is needed)
1-camettWayblll NUmber
I I
Special InstructionS/
Containers & ~~ j Conditions ot Receipt Matrix Preservatives l o r~ ! ~ I • l ~ .., ~~~ ::.I= ~ rme ~ ~ ~ ~ .,_ '--
15:00 ' ix IX lx I \Y\b'-\~\s
'' ' L--' I I r----r J D I ,___
~r~
CJ
I
'1 ' .
' -
Possfbi9 HazsnJ 1dfmllfica/ion I~ D/!Jpos>ll PI teerriay~-~u~-111!1 Tf!lafnsd 0 Non-HBzarrl 0 Flammabls 0 Sfdn 111i1B11t 0 Poison B · 0 Unknown 0 fWtum To CHent 0 D/$polla/8y Lab D Atcfllvtl For --Months lct!gMfllBn 1 month;
TumAiolmtJ Tlm9 ~ret/ ·OC lieqtmmerrtS (Spe::ify)
0 24 flot.tJs· D 48HOUIS 0 7De.ys 0 14Dsys 0 21 Days o 0/tiet'. Las.ooc.metbhu --(;ln:iJ ~~/b;.--I Da~ 111ilfe I {,-en-1'3 1-z.:oo 1~ }J::J. \\:Q, 0i -~f\-U !t\~-r~ 1
Tnne
\2.4c:;
2. ... y I Delle
1
Tnm~ 2.fboclve:dBy ' lOaM ll'Jms -""'
3. Re5nqufs/led8j ,~ l'llmll S.RQcan.edBy Ia. 117ine
Camim!l'>ls _ _ _ _ _ .. I When. Complete Email to: pean or Paul [e-mail] . _ _. _ _ _ -I
DIS1fi/Stm0N: Wl';lfTE-~to Cii.w wil1l Fll>pQit: CANARY-S!'ltl'$ with '1M SiiiilpJt>; PINK-FIB/d CiJiiY
--------·-----------------------.
Sample Check-in List
Container GM Screen Result: (Airlock) _l.lo_cpm Jnftial~ ]
Sample GM Screen Result (Sample Receiving) ~cpm Initials ]
1....\l..._Q(\ <{.'-\ . SAF #: Nt\ ] Client: \ . f:0 SDG #:
Lot Number: -s'~(. \ "'&-D '-\
Chain of Custody# ________________ --------------------
Shipping Container ID or Air Bill Number : ______ -------NA ~ )
Y cs ~ ] Continue with 1 through 4. Initial appropriate response.
No [ ] Go to 5, add comment to #16.
Samples received inside shipping container/cooler/box
1. Custody Seals on shipping container intact?
2. Custody Seals dated and signed?
3. Cooler temperature:
4. Vermiculite/packing materials is
Yes [ No[ No ~..ustody Sea~ l
Yes [ No [ No C\1stody en] ,~ ]
oc NA~ )
NA[ Wet [ ] Dry~ ]
5. ChainofCustodyrecordpresent? Yes ] No[ ]
Item 5 through 16 for samples. Initial appropriate response. ~
6. Number of samples received (Each sample may contain nml 'iple bottles):._\.!._ ______________ _
7. Containers received:~~~ :$.-b~.~-=----------------------
8.
9.
10.
11.
12.
13.
14.
15.
16.
Sample holding times exceeded? NA [ Yes [ ] N J
Samples have: __ tape __ hazard labels cu ·tody seal ~propr~ate sample labels
Matrix: ~A (FLT, Wipe, Solid, Soil) __ I (Water) ~S (Air, Niosh 74 0) ' T (Biological, Ni-63)
. an1ple ·~· ~ \o-'<¥-'~
are in good condition , __ are leaking __ arc btol<e~
__ have air bubbles (Only for samples requiring no head space) __ Other -----------
Sample pH appropriate for analysis requested Yes [ ] No [ ] NA ~ ]
(If acidification is necessary go to pH area & document sample ID, initial pH, amount of 1 I~3 added and pH after addition on table)
Were any anomalies identified in sample receipt? Yes [ N~
Description of anomalies (include sample numbers): N~ --------------------
Sample Location, Sample Collector Listed on COC? *
*For documentation only. No corrective action needed.
Yes [ ] N~
Additional lnformation:~·J-11!:>!.------------------------------
] Client/Courier denied temperature check. ] Client/Courier unpack cooler.
Sample Check-in L-i Signature:·----~¥--..b<o"""'-~~~..z'----------Datc.;: \.o-\\ _..\)
Date:
By:
Person contacted: [,Xi No action necessary; ~rocess as is
ProjectMon!tgiJr~~
LS-023 Rev. 17,05/13 Page 1 of-\-
TestAmerica Laboratories, Inc. 12
APPENDIXD
South Yell ow Cake Scrubber
Figure 1. Facility Schematic Representation
Yell ow Cake Dryer Baghouse
Figure 2. Facility Schematic Representation
Grizzly Baghouse
Figure 3. Facility Schematic Representation
Production and Control Equipment Data
South Yellow Cake (Scrubber Flow Rates)
Yellow Cake Dryer Baghouse (Delta P readings on Field Data Sheets)
Grizzly (tph of material and belt speed)
D
Fadlity Energy Fuels Resources
t
a
t
y
stackidentification: South Ye ll ow Cake Scrubber
l+--0~1
~
~: Distance downstream from last disturbance, feet
y: Distance of Sample Level to Ground, feet _
0: Stack Inside Diameter, inches __
Estimated Moisture, percent
Estimated Temperature, °F -----
Estimated Velocity, fpm __ _ ~------
Control Unit
Type:
Scrubber
Number ofPorts
~
Figure L Facility Schematic Representation
Process
Type:
Yellow Cake Processing
Focility, Energy Fuels Resources
t
a
l
y
Stack Identification: yell ow Cake Dryer Baghouse
l+--0-+l
~
a: Distance upstream from next disturbance, inches
~: Distance downstream from last disturbance, inches
y: Distance of Sample Level to Ground, feet
0: Stack Inside Diameter, inches
Estimated Moisture, percent
Estimated Temperature, °F
Estimated Velocity, fpm ___
Control Unit
Type:
Baghouse
Number of Ports 2
57"
454"
65'
16"
0-2%
125
1,400
Figure 2. Facility Schematic Representation
Process
Type:
Yellow Cake Processing
F•dHty, Energy Fuels Resources
t
a
!
y
stackidentification: Grizzly Baghouse
l+--0-+l
~
~: Distance downstream from last disturbance, inches
y: Distance of Sample Level to Ground, feet _
0: Stack Inside Diameter, inches . -·
Estimated Moisture, percent
Estimated Temperature, °F _ _ ----·
Number of Ports
Process
Type:
Control Unit
Type: ,...._.._ ______ --i Ore Unloading and Conveying
~
Baghouse
Figure 3. Facility Schematic Representation
Energy Fuels Resources, Blanding, UT Process Data
Source: South Yellow Cake Date: Lf /; 7r 3
Scrubber Flow GPM
Time #1 #2 ~p
T .'3D 10-4 I(J·7f
f.; O() ~c) ·I l Q ·1-
¥:'3o .., \.0 I c)'-:).
q:,.--0 0 ~\-'\ l D ·--;}-
~ ."3 {) "> \ ·\ l u . "1---
'(.) : OD ·?,) -(.'> r : \ ~ ~~~ -' . : { l • :
[D • . 3D "/ ' ,) I ! \
.,
~;~t t ' ' \ ~ •' /I
I~.' OD . ' 1
~ I A 'J
I . r' . ! • ' •'• ., I ~) ---,, .:
i _,.··) ... (~) C'J I "' ">',, ; .. () l ' . 'I .
• .-I "/ ~) ->i·~ ro ·1--! i )
I
\ . ~'Z· '1..-( () .-:;. r •' .
~-· / .:_ "'\ 71, . ~ (D ~-+ J I
I c.( (.)0 ~r 0 \ D 'f
\vi ~ >t> ~ "S-3 (0'4 >J• -J
\~: oo ~ ~ ·) [ () ·1 . )D )7· "L (5" . L fl ~1-
I oD ti.P. -; 7 . \ l D·1
Energy Fuels Resources, Blanding, UT Process Data
Source: South Yellow Cake Date: 4 ~/ ()
Scrubber Flow GPM
Time #I #2 t-P
1.'~ D 5?. .')-' t (>. 1-
¥':c)D ~1· ~ ft r11 -=i
~: 3 () )1-' v \ 0·1-
~ : ()(.;> 71·'1 ~ /D·~~
q. 36 ~ \· ~ ro·-1-
tO·. Do )-z..·7 tv· t
{6: '?a 11-· \ (()·1--
1 r ; oo 7t·~ (b·f---
vi : 10 21-·1 ( 0·~
I z. : QO ~z.L\ lo-1---
12. : '0 ~ '{. -s I o · -:f
,, ·. oo )Z.lt) (;D . i
3. ) 0 I . ,1.(o ro·Sf-
\c.{_'CJO ~1.--D /b ·1
( y :50 7z·7 \0.~
. 0 C>
l 5"" -)1·--{ 1 c. 1-
rs-·. 3o '2 ~. ~ (n ·1
,.
Energy Fuels Resources, Blanding, UT Process Data
Source: Grizzly Baghouse
Time
/ ,/ I"$ '. ) J . / t fa. I)
I b · 3)
' / / \(, 'j (
t"l '1\ (
\-{·, 3 (
ll', { )/
..-/ I~~/)
1\?J'.)(
IB'.:)f'
l9 ·. , -r~
l'i '.j)
1 '. 3 8
t?: ov
B. ~D
6: ~0
1 I ~ o()
'1 '. LO
9'140
IO>oo
\0 ·. 2.-D
tO'. L{O
I I :oo
t l '. ') q
Tons (Integrator)
(pI {L{ IO
Lll'-l7o
lo 1152.f'
fotl 5·7)
/' &lt ls3l
~II ~q o
~Ril 11o
/
<o ll <bo)
~dtl tO~o
/ ~/191'J
~ tl q 7)
{o 1L03 0
~1'3!70
La I~ L3J/-
L,13 -z_qo
(p 1·3 )Y)
/ ~t7YoJ
·"" 01) L/Y)
G,i-:J5o) /
fot~)555
<ol3(oiJ /
~1)(,10
l9 [ ~·l "L (
l11 1 ~ lc;O
Date: ~ (5 -c, lt3
tph fpm
\2.6 l08.'1'
\ L) l 0 8.((
\ l j \ eli( 'D
.... ~ I Ll j l 0 8 I C(
l0f L o'1, (
t ~ 0 IOB·b
\ z._( 10£3,·-r
ll-\) /08r-~{-
\{) I ot], (
~~r log.~ ·-jOC,r\3 I y J
tf) l08· 9
\ ·'":S 0 l 0 ~·(t'
{ 3 0 lo6 .q
t) f/ )09.0
10 r.,., Jo8/T'
r I z... J 1o6,9'
/'L 0 /08( -=!-
I L(O to9.o
13 D 1oB~1~
I ?f' lo6~-+
---;;;;;'
APPENDIXE
Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature
sensors were carried out in accordance with the procedures outlined in the Quality Assurance
Handbook. The appropriate calibration data are presented in the following pages. The nozzle
calibrations are recorded on the first page of the field data sheets.
Figure 4 Schematic ofMethod 51114 Sampling Train
Meter Box Calibration Data and Calculations Forms
Post-test Dry Gas Meter Calibration Data Forms
Type S Pitot Tube Inspection Data
Sample Box Temperature Sensor Calibration
E
Temperature Sensor
t ~-·
TypeS Pilot
Tube
Te~~~~r:e _
Gooseneck I . Nozzle t-WTraced ~ ~
/•Rd:e .--------..
/
TypeS Pitot
Tube ~
Temperature
Sensor
Glass Fitter
Holder
Heated Area
lrJlllngerlrain C;l~onat, MayBe Replaced
8t An Ettulvalent Condenser
j
,--·--------=----lmpingers
Stack
Wall Manometer Temperature Water Sensors. Empty Silica
Gel
Orifice
Dry Gas
Meter
Figure 3 Schematic of Method 5/114 Sampling Train
Vacuum
Line
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.
2) Record barometric pressure before and alter calibration procedure.
u-~~....... --.. ~-/J.: -~-~-: r .
3) Run at teoted vacuum (from Orffice Calibration Report). for a period of time
nece•sary to achieve a minimum total volume of 5 cubic feet.
4) Record data and information in the GREEN cells, YELLOW cells are calculated.
METERSERIAL#:I -·y~ I
CRITICAL ORIFICE SET SERIAL#: 1453S EQUIPMENT ID #:
K' TESTED
,.-----.----l FACTOR I VACUUM
G
G
G
RUN# I (AVG)
0.81:17
2 0.8t31
0.111.3.7
0.5317
2 O.&li7
3 0.5317
0.3307
2 !1.3307
3 0.3307
(In Hg}
13
13
13
13
13
13
13
1:1
13
645.807 852.11$
852.115 658.605
G58.60& , 665.0!1&
BOZ.DD3 607.809
&tl.D65 BtU!$
618.669 824.268
628..000 633,184
833.184 6311..396
538.396 643.626
USING THE CRmCAL ORIACES AS CALIBRATION STANDARDS:
8.508
6.490
6.461
5.606
5.604
5.599
5.184
5.212
5.230
71 78
71 79
71 79
69 7l
69 74
6!1 75
71 72
71 73
71 76
79 84
79 87
19 87
74 l$
15 76
75 n
73 75
75 110
76 80
87
87
87
76
n
78
80
so
80 -~
DGM
AVG
82
8l
83.00
74.50
75.50
76.25
75.00
77.25
78.00
FINAL
I 25.20 I
ELAPSED
TIME(MIN)
e
AVG(P,")
25.20
§§.60
2..60
2.60
MD § 0
0
E§ 40
40
12.00
12.00
12.00
.uill.
5.3564
~
!l&M
llHl
~
4.31411
~
~
2013 Pre-Calibration
IF Y VARIATION EXCEEDS 2.00%,
ORIFICE SHOULD BE RECAL!BRATED
1
~ ~
5.3407 .Ml!1.
~ .tw.
AVG= Mll .:9JP.
!&ill. ~
~ ~
Mill lJ!Q1
AVG= ~ ~
4.3411 1.006
~ Lm!!
Ulli LQlll
AVG= .1&Q! 11M
~
Mll
.till
.!.ill
1.518
1.516
.1&1
~
.Mll
The foHowing equations are used to calculate the standard volumes of air passed through the DGM. V0 (std), and the critical orif~.
V" (std), and the DGM calibralion factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = r:I¥0 :J
(1)
(2)
(J)
Vm<""; = K, • Vm• Pbar+(!lH IJ3.6j
Tm
Vcr,,,.,; = K '• !_l}_ar " e Jl"'",;mb-
= Net volume of gas sample passed through DGM, corrected to standard conditions
K, = 17.64 'Riin. Hg (English). 0.3858 'Kimm Hg (Melric)
T m = Absolute DGM avg. temperature ('R -English. 'K ~ Metrie)
= Volume of gas sample passed throug/1 the critical orifice, corrected to standard conditions
T arr.b = Abscfute ambient temperature (eR-English. °K ·Metric)
Vct(:rd) Y= .-v·m1 .. rd,
K1 = Average K1 factor from Critical Orifice Calibration
= DGM calibration factor
Ice Bath
Ambient Air
Sorting Water
AVERAGE~H~=r: f.49JC:)
2 ~H~: ( 0.75 9 ) 6H (Vm(std))
Vc,(std) Vm
Temperature Sensors
Reference In Out
OF OF OF
33 33 33
62 62 62
202 203 203
PRE Console #4 Calibration 2013
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.
2) Record barometric pressure before and after calibration procedure.
'& ... , ... _ -"';}!;.. ... ~ .
::x:--r -i~~ u ~· .. -:· .. -
3) Run attested vacuum (from Orifice Calibration Report), for a period of time
necessary to achieve a minimum total volume of 5 cubic feet.
4) Record data and information in the GREEN cells. YELLOW cells are calculated.
METER SERIAL M:l ..... I
CRITICAL ORIFICE SET SERIAL lr: 14535 EQUif'MENT ID II:
K' TESTED
r-------.---~ FACTOR IVACUUM
G
G
G
RUN# I (AVGI
2
3
z
3
2
' 0.8137
O.IJ137
0.8137
0.53·17
0.53'7
O:S~11
0.3307
0.3307
0.3307
lin Hgl
1Z
12
12
13
13
13
~
ZD
111
12l!.Z04
133,588
139.DZO
95.7570
100.951
108.478
111.900
117.fti8
122.339
USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
133.588
139.020
144.448
10o.951
1.015.47.9
111.4$8
111.1os I
122.339
127.559 I
5.384
5.432
5.428
5.194
5.628
5.219
5.208
5.231
5.220
70 76
70 83
~-86
~ ~
~ ~
-~ ~
70 ,74
70 76
70 16
83 78
85 84
86 93
~ y
m n
h ~
75 75 ,. 78
77 77
84
93
il4
n
n
~
78
77 _
7.S
DGM
AVG
79.75
88.25
89.50
59.75
70.75
72.50
75.00
76.00
76.75
FINAL
~·I
ELAPSED
TIME(MIN)
9
AVG(Poul
25.45
§§60
2.'80
2.60
7.50
a,oo
7.50
u.oo
12.00
12.00
l§ 40
40
~
~
4,4705
~
~
~
~
4.3889
~
2013 Pre-Calibration
IF Y VARIATION EXCEEDS z.oo•A.,
ORIFICE SHOULD BE RECAUBRATED
l
~ .Q,lli,
4.4890 ~
4.4990 1..m
AVG= .1&ll Mi.
~ ~
!1m 1.D!Ii
~ .un
AVG= ~ .:!ill.
4.3883 !.ill
~ ~
~ 1,W.
AVG= ~ w
The following equations are used to calculate the standard volumes of air passed through the DGM, v •. (std), and lhe critical orifoce,
V~ (slrl), and the DGM calibratbnfactor, Y. These equaiions are aulomatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y = I 1.001 I
(1)
(2)
(3)
Vmt"'"' = K, * Vm • Pbar +(~H I 13.6)
Tm
Pbar "El
Vcr,,.,,, = K'* .JTamb
= Nel volume of gas sample passed through DGM, corrected to standard conditions
K, = 17.64 'Riin. Hg (English) 0.3858 'Kimm Hg (Metric)
Tm =Absolute DGM avg. temperature ('R-English, 'K-Metric)
"Volume cf gas sample passed through the critical orifice, corrected to standard conditions
T.;nb = Absckrte ambient temperature (0R-English, °K-Metric)
Vct;Ttd) Y= -
Vn1pid1
K' = Average K' factor from Critical Orifice Calibiation
= DGM calibration factor
AVERAGE ~HI!"' 1.481 I
I ~H~J" ( ~) 6H (Vm(std))
V0,(std) Vm
Tempereture Senaors
Reference In Out
'F
32
72
203
'F
33
73
202
'F
32
73
202
1.lli
~
1.488
.Lill.
1.lli
1.,.ill
j,lli
Mn
1d.lQ
Pre 2013 5 console
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES ~-~~· '£Is !&W*' /&&11!!--~·!!!..;;::-
1) Seiad lhree critical orifices to calibrate the dry gas meter which bracket the expected operating range.
2) Record barometric pressure b2fore and after ca~bration procedure ENVIRONMENTAL SUPPLY COMPANY
3) Run at tested vacuum (from Orifice Calibration Report), far a period of lime
necessary to achieve a minimum total volume of 5 cubic feat.
4) Record data and information in lhe C,fiO:Et< ceHs. YELLOW cells are calctJialed,
METER SERIAL ''] ····-~· I
CRITICAL ORIFICE SET SERIAL !I< 1453S EQUIPMENT 10 #:
K' TESTED
~--~~--l FACTOR I VACUUM I I RUN# I (AVG) (in Hg)
0
G
G
~
3
2
Q.8"l37
O.IU7
a.eur
0J&:l17
OJ$:)17
o.un
Ul07
Q.J307
0.3307
~z
·12
12
1:Z
t2
12
u
12
13
40LU9
411:914
4!7.614
UUQ:I
3t3.27.1
3118.1S~
424.551)
.H.IISt
435.011
USING THE CRLnCAL ORIFICES AS CAUBRATIDN STANDARDS:
4.1U64
417.814
4~U74
3P.L2Tt
3H.i3l
403.8'114
4JUI1
4:15.011
440.174
6.381
5.8&0
5.810
5.1&8
5.211
&.162
6.331
5.130
5.163
70 1&
70 18
70 10
TJI 72.
70 72
70 __!!___
7:5 .71
7& 17
75 78
78 73
10 74
11 74
·72 .u
71 n
L_~ 72
77 14
78 74
71 74
74
14
74
lZ
72
7Z
74
74
74
DGM
AVG
75.25
76.5
77.25
C4.50
72.75
74.00
71.50
7&.75
76.00
FINAL AVG (P.,,)
I 2&.20 I
ELAPSED
nME(MINI
9
25.20
§§.00
3.00
3.00
§§§.zo
1.20
1.20
§ 44
44 12.00
u.so
12.00
2013 Pre-Calibration Console 9
.u.m
!.UH
Yill
~
Mill:
Yl!fl
i.m!
~
4.281S
IF Y VARIATION EXCEEDS 2.00%,
ORIFICE SHOULD BE RECALIBRATED
l
Y£ 2.Hi
uooz !..Ml
Yl!U LW
AVGz .1..9.21 :!!.ll
~ lto!!l
~ U!1
~ l.W
AVG= un ::R.H
.4.RR 1.W.
~ 1.lli
!.ll9. .t.m
AVG• !.ill. l!.H
1.1U
1.IZ!
ill!
!.W.
!.W
.1.W.
1.W.
~
1.m
The following equations are used to calculate the standard volurMs ol air passed through !he DGM, V. (std). and lhe critical orifice,
V,(std), and the DGM colibralionfaclor, Y. These equations are automalicaNycalculatod in the spreadsheet above. AVERAGE oRv GAs METER cAueRArloN FAcToR, v = C1-:-oo4 I
(1)
(2)
(3)
Vm..,,,, = K, • Vm• Pbo>--rltVf Jt3.6)
Tnl
Pbw •e Vcr .. ~,.,, = K'• .JTamb
= Net volume of gas sample passed through DGM, corrected to standard conditions
K, = 17 64 •Riin. Hg (Engll<hl. 0,3858 •1</mm Hg (Metric)
T"' .. Ab$Ciute DGM avg. temperatull! ("R -English, "K ~Metric)
=Volume of gas sample passed through the crllical orifice, corrected to standard conditions
T wb = Absolute ambient temperature (~R-E;;gli!h, •K-Metricj
K' = Average K' factor from Critical Orifice C.oalibration
Vcr(rJdJ Y = -Vnt,,,.,1
= OGM calibration factor
AVERAGE.<!.~ =f:U79 I
2 Mi~ = ( 0.75 8 ) .<l.H (Vm(ald))
V.,(sld) Vm
Temperature Sensors
Reference In Out
"F OF OF
32 33 33
72 73 73
201 202 203
Console 9 Pre-test 2013
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. r' @Mfrli&*UM/IW ~~ 9 ~~ -'" 2) Record barometric pressure before and after calibration procedure.
3) Run at tested vacuum (from Oririce Calibration Report), for a period of time
necessary to achieve a minimum total volume of 5 cubic feel
4) Record data and information in the GREEN cells, YELLOW cells are calculated.
METER SERIALII:I -· ---I
CRITICAL ORIFICE SET SERIAL II: 1453S EQUIPMENT ID #:
K' TESTED
.-----.-----1 FACTOR I VACUUM I I RUN# I (AVG) (in Hg) INITIAL FINAL
0:-~~ L:J3 ~ G±=j
.0
.0
.0 I I I I I I
G:
r:l:~~ L:Jl~ G±=j
0.5317 13
0.5317 13
0.5317 13
658.541 666.591
6&8.591 672.794
872.7M 878.388
USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
7.050
6.203
5.592
.0
.0
.0
75 I 80 82 80 83
75 l eo 82 81 83
rs _l a1 82 83 84
1-I I I l l
DGM
AVG
0
0.00
&1.25
81.50
82.50
0.00
0.00
0.00
Facility :
FINAL AVG (P.,,)
I 25.30 I
ELAPSED
TIME (MIN)
a
25.30
§§
1.10 § 00
00
§§
5.83$1
5.1311
4.611§
Energy Fuels
IF Y VARIATION EXCEEDS 2.00%,
ORIFICE SHOULD BE RECALIBRATED
AVG=
5.8175
Uill.
~
AVG=
AVG=
0.9!17
~
.1JlQ§
~
1
~
!,ill
~
~
The following equations are used to calctJiale the standarn volumes of air passed through the DGM, V m (std), and the cntical orifice,
Vg (std), and the DGM calibration factor, Y. These equalions are aulomaticallycaiCtJiated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, y =I 1.008 I
(1)
(2)
{3)
Vm(uil = K1 • Vm• Pbar+(t1.H /13.6)
Tm
Pbar * 8
Vcr,,w) = K'• .JTamb
= Net volume of gas sample passed through DGM, corrected to standard conditions
K, = 17.64 •Riin Hg (English), o 3858 •Kimm Hg (Metric)
T m = Absolute DGM avg temperature ('R-English, •K-Metric)
= Volume of gas sample passed through the critical orilica, corrected to standard conditions
T .me = Absolute ambient temperature ('R-En!Jiish, ~ • Metrlc)
K' = Average K' factor from Critical Orifice Calibra\ion
Vci(Jrdi Y= -
Vm(sld)
= DGM calibration factor
Ice Bath
AmbieniAir
Boiling Water
AVERAGE~~~=[ 1.512 I
2
IIH@: ( 0.75 a ) IIH (Vm{std))
Vc.(std) Vrn
Temperature Sensors
Reference In Out
°F "F "F
33
62
202
33
62
203
33
62
203
Post Console #4 Calibration 2013
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.
2) Record barometric pressure before and after calibration procedure.
3) Run at tested vacuum (from Orifice Calibration Report), for a period of time
necessary to achieve a minimum total volume of 5 cubic feet.
4) Record data and information in the GREEN cells, YELLOW ceNs are calculated.
METER SERIAL 11;1 -----I
CRITICAL ORIACE SET SERIAL /1: 14538 EQUIPMENT ID II:
K' TESTED
r------r---1 FACTOR I VACUUM I I RUN II I (AVG) (in Hg)
D:~E§ .0
.0
.0 F I I I -1 I
G: o.e317 12 ~
' 0.6317 12 I
0.5317 12 I
861.050 866.129
868.129 871,60
aru;o Bn.442
D:~E§
USIMG THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
5.079
5.471
5.642
.o
.0
.0
113 58 60 60 62
63 60 62 62 66
8J e2 611 64 1!5
I-I II II
DGM
AVG
0.00
0.00
0.00
59.50
62.50
54.25
0.00
0.00
0.00
FINAL I 24.85 -1
ELAPSED
TIME(MIN)
9
AVG(P,,.)
24.1!5
§§
§§ 00
50
§§
4.3022
4,8076
~
Energy Fuels
IF Y VARIATION EXCEEDS 2.00'/o,
ORIFICE SHOULD BE RECALIBRATED
AVG=
~ !J!!!I
~ ~
~ U!!!Z.
AVG= ~ M!!
AVG=
~
1M!!.
.Lill
The following equations are used to calculate the standard volumes ol air passed through the DGM, V m (std), and the critical orifice,
V" (std), and the DGM calilirlltion factor, Y. These equations are automatically calculaled in the spreadsheet above AVERAGE DRY GAS METER CALIBRATION FACTOR, y = (1.004 I
(11
(21
(3)
Vm1,dJ =K, •Vm•Pbar+(Mil1J.6)
Tm
Pbar •0
Vcr,,.,J = K'• .JTamb
= Net \/Oiume of gas sample passed through DGM, corrected to standard conditions
K, ~ 17 64 'Riin. Hg (English), 0.3658 'Kimm Hg (Metric)
T m ; Absolute DGM evg temperatura ("R · English, 'K • Metric)
= Volume of gas sample passed tihrough the critical orifice, corrected to standard conditions
T, .... ; Absolute ambient temperatura ("R · English, 'K ·Metric)
K' = Average K' Factor t:om Critical Orifice Calibration
Vcr(.rrdJ Y = -
Vm(sllit
" DGM calibration factor
AVERAGE aHa =I 1.561 I
2
<1Hg = ( 0.75 B ) <1H (Vm(stdl)
V.,(atd) Vm
Temperature Sensors
Reference In Out
OF
32
72
203
•F
33
73
202
OF
32
73
202
post 2013
r: --~~=
9 Q&!iii·AII·"'AM.n&i~' ~
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES
1) Select three critical orifices to calibrate the dry ga• meter which bracket the expected operating range.
2) Record barometric pressure before and after calibration procedure. ENVIRONMENTAL SUPPLY COMPANY
3) Run at tested vacuum (from Orifice Calibration Report), for a period of time
necessary to achieve a minimum total volume cf 5 cubic feet
4) Record data and information in the GREEN cells, YELLOW cells are calculated,
METERSERIALij:l ·-· ----~
CRITICAL ORIFICE SET SERIAL II: 14535 EQUIPMENT 10 II:
K' TESTED
.-----.-----l FACTOR I VACUUM I I RUN II I (AVG) (in Hg)
DEBE§ .0
.0
.G I 111 -D
0: 0.6808 12
0.6808 12
0.6808 12
546.903 551.219
551.219 655.955
!556.185 562.719 I
DEBE§
USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:
5.316
5.746
5.754
.D
.G
.D
62 65 66 60 65
82 68 611 85 66
82 68 TZ . !!___ 67
[ lll _l_l
OGM
AVG
0
0
0
64.00
66.25
88.25
0.00
0.00
0.00
FINAL
[ 2;;]
ELAPSED
TIME(MIN)
9
AVG(P..,.)
24.85
§§
§§ 50
60
§§
4.4761
4.8174
~
Energy Fuels
IFYVARIATION EXCEEDS 2.00%,
ORIFICE SHOULD BE RECALIBRATED
AVG=
4.4442
4.§145
~
AVG"
AVG=
~
Qm
~
~
1
QJ!Q
The following equations a~ used to calculate the standard volumes of air passed through the DGM, Vm (sld), and the critical orillce,
v .. (skl), and the DGM catibration fac1or, Y. TheSl! equations are automaticafty calculated in the spreadsheetabcve. AVERAGE DRY GAS METER CALIBRATION FACTOR. y = c-o.sga 1
(1)
(2)
(3)
Vm1,.,1 = K, * Vm * Pbar + (M /13.6)
Tm
Pbar •e Vcr, • .,, = K'• .JTamb
: Net volume of gas sample passed through DGM, corrected to standard conditions
K1 ; 17 54 'Riin. Hg (English), 0.3858 'Kimm Hg (Metric)
T m = Ab&Oiute DGM avg. temperature ('R ·English, 'K ·Metric)
" Volume of gar. sample palr.sed through the critical orifice, ccrrected to standard ccnditions
T.,., = Absolute ambient temperature ('R ·English, 'K · Metric)
K' ; Average K' lacier from Crilical Orifice Calibration Vc'iml) Y= --= DGM calibration factor
Vm,,MI
AVERAGE t.H<m ,, 1.719 J
1
t.Hill" ( 0.75 e ) t.H (V.,(std))
V.,(atd) Y.,
Temperature Sensors
Reference In Out
OF OF OF
32 33 33
72 73 73
201 202 203
1JlZ
1.Z1!
1211
Console 9 Post-test 2013
.::d' p; /,y (-'~------.. ---..
'· --......~
~. B:
_ .. --
--:7-3-~ 1'.' ~-=-;_;:. __ ::-E3 ·-·--;. __ -
"· ·····~·-· 0
-~ ;!;-:-~;~~:.!!..:~..­
~·)L.r.:e
D;no
r,, < j'
~: < s'
z ~ (l 1:!5 ir:
\\·::;_~:~0~1~5ir\
\\' > .-:. ir..:h~~
Z.> 3-! ll.dl
l,; 1\ = Pn '! 'C-S -+---='----1,: 1.•)5. D, ~ D, s 1 ~.). D, '? Yv&
'":= __ .....:.... __ _
";=--~---
(i, = __ _!'Z....:.._ __
[1: = __ t..-=---~
z = ----''_;;:()'--0-' _i:-.
\'"-. -. oo l ic
II = (p 'tz... In
Z= IC
y ~ _3_~-""'---'"'
ICE 1'.'-\Tt:': ~-' I "c.J ![ \
~ILJCO\~ 0!:.
c-.
I ~---~ ~.---" ./ ~ n. ~~ ~------~ ~-~ -......... 1 p:: ' , -
..
;·--A l) c,
·8 .... } ·~
T~ p~ S Pi tot ·r ubc lnsp~ction Dat::
D:= .> 1.(
.:.-~'•:_~ _ __:.•_:4:3-..::t.t~t>~--'"
,:_:_: •_' _. _l.f.:_4__;_,::0:..,.___ ,,-
C: < s'
Z::;0\~)1;~
\\' .5 •)03t2S in.
'-':= 7,.-
r<;= 0
P:= ______ _
z~ . f)l'"] i ;~
W= .0 l5" u:
\\' ~ -, In
z~ lr.
__J I ) ~ I" --~--··
l ~·:r:~::~::1r.:
!):;':'::""''
(II
$1LICW\E Oli.. ~
T~p~ S l'itot Tube \n:;pcction D:1::1
D~:e 11 -I l -\_1__
D:= • .3 , $" i~
f',o, • g.c, 0 I~
..:.....i\_~ __:.•:._'f.:..:!C47~0 __ "'
(;," 1')
C:; :::---'----
ll: ~ __ .t;.__ __
z o: (! lc5 in Z= • 0~1, 1:'· .
\\' :;_ ..-y 03 1~) in ,,,· = . co~ If.
{o
\1 ~ ;r:
l > 3 ~: in.:h Z= tY, -7 1::
£--r-I. ........ . ( ~)
,\IR I) "l '1.-1. .,_. I o
~\I !CO\E 01!
TETCO
Sample Rox Temperature Sensor Calibration
Date: 12/19/12 Calibralor: Mike McNamara Reference: Omega CL3512A
Thermocouple Temperature Temoeraturc Temp. OifT.
Unit ID Source Reference Sensor or Result Location (Medium) tF) (''F) (•l'l, P/F
Oven Water 33 34 I
Water 204 204 0
A Probe Out Water 33 34 1
Water 204 204 0
Impinger Out Water 33 34 I
Water 204 204 0
Oven Water 33 35 2
Water 204 204 ()
B Probe Out Water 33 35 2
Water 204 204 ()
lmpinger Out I Water ~ 33 I 34 I
Water 204 204 ()
Oven I Water I 33 34 I
Water 204 204 0
c Probe Out Water 33 34 I
Water 204 204 0
lmpinger Out Water 33 34 I
Water 204 204 0
Oven Water 33 33 0
Water 204 204 0
D Probe Out Water 33 33 0
Water 204 204 0
lmpinger Out Water 33 34 I
Water 204 203 -I
Ovl!n Water 33 34 I
Water 204 204 ()
E Probe Out Water 33 34 I
Water 204 204 0
Impinger Out Water 33 34 I
Water 204 202 -2
Oven Water 33 34 1
Water 204 204 0
F Probe Out Water 33 34 I
Water 20 204 0
lmpinger Out Water 33 35 2
I Water 204 202 -2
IL "' Water 33 34 1
llftu lmpingcr Out G Water 204 202 -2
lmpinger Out H Water 33 35 2 < I
~ Water 204 202 -2
I ~ -Water 33 34 I Impinger Out I
~~-Water 204 204 0
·' lmpinger Out J Water 33 34 I
Water 204 203 -I
~-Water 33 34 I lrnpingcr Out K Water 204 204 0
·~C'
I
APPENDIXF
The testing followed the same procedures as outlined in previous protocols and tests at this
facility.
ATTACHMENT H
SURFACE WATER GRAPHS AND FIELD DATA SHEETS
1.00E-05
1.00E-06
1.00E-07
-..!
ftl ~.OOE-08
l:n 0 ..J -
1.00E-09
•• •
• • . -•
-M.-.-
1.00E-10 .. ---
1.00E-11
OJfQI),
~-;.;;. ~
-
----
~ ';).~OJ ~~
Cottonwood Creek Dissolved Radionuclide Concentrations
(uCi/ml)
~
• • •
• • .. • • • -
-
•
•
-
-
..
•• • • ••••• • ••• . .._...._._. ........ __
£ ·-
OJOJI),
~-;.;;.
~~"
-
'
R>fQ ~~Oj ~fd
~~~
rV" ~~"
I • U-Nat. • Th-230 & Ra-226 ]
~OJ ~ <,}~OJ
• •
A
~
----~~ f}~
~"
1.00E-06
1.00E-07
1.00E-08
-Cl)
(ij ~.OOE-09
tJ)
0 ...J -
1.00E-10
1.00E-11
1.00E-12
~<t:>
-:.."OJ ~"
... ,.. •
• ---•
~ ~..._OJ ~~
Cottonwood Creek Suspended Radionuclide Concentrations (uCi/ml)
•
... -• -
A ....
... •
& -· • '""' •• .... • A
... .... • • • -... ... • • • • •• ·-................... • •• •
A
-
' '
B~ Bn;, B<t:> Bco ~" ~ ~co ~OJ ..._€), ~ ~..._C!J ~"C[) ~..._C!J ~..._C!J ~ ~ ~ ~f),~ ~ ~
~~ .... ~ ~'<) ~.-,; ~ ~..._OJ n}.-,;
~cv n}.-,; ..._')) ~ ~ "" q}'l; ~"
! •U-N~•Th-230 £Ra-226 1
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax:[phone]
e-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Garrin Palmer
Energy Fuels Resources, Inc.
6425 S. Hwy 191
Blanding, UT 84511
TEL: [phone]
RE: 1st Quarter Surface Water
Dear Garrin Palmer: Lab Set ID: 1303553
American West Analytical Laboratories received 1 sample(s) on 3/22/2013 for the
analyses presented in the following report.
American West Analytical Laboratories (A WAL) is accredited by The National
Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is
state accredited in Colorado, Idaho, New Mexico, and Missouri.
All analyses were performed in accordance to the NELAP protocols unless noted
otherwise. Accreditation scope documents are available upon request. Ifyou have any
questions or concerns regarding this report please feel free to call.
The abbreviation "Surr" found in organic reports indicates a surrogate compound that is
intentionally added by the laboratory to determine sample injection, extraction, and/or
purging efficiency. The "Reporting Limit" found on the report is equivalent to the
practical quantitation limit (PQL). This is the minimum concentration that can be
reported by the method referenced and the sample matrix. The reporting limit must not be
confused with any regulatory limit. Analytical results are reported to three significant
figures for quality control and calculation purposes.
Thank You,
Approved by:
F • Digfially signed by Kyle F. Gross
ON: cn=Kyle F. Gross, o=AWAL,
ou=AWAL-Laboralory Direclor,
email=[e-mail], c=US
Date: 2013.03.27 16:08:12 ·06'00'
Kyle
Gross
Laboratory Director or designee
Report Date: 3/27/2013 Page I of7
All ana1yses applicable to the CWA. SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the altached COC This report is prO\ided for the exclusi'e use of the addressee Privileges of
subsequent use oft he name of this com pan~ or any member of its staff, or reproduction ofth1s report in connection \\llh the ad\'ertisemenl, promotion or sale of an) product or process. or in conneclion "ilh the re-publica! ion of this repor1 for any
purpose other than for the addressee \\ill be gran led onl~ on contacl. This company accepts no responsibility excepl for the due perronnance of inspection and/or anal~ sis in good faith and according lo the mles of the trade and of science
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: (80 I) 263-8687
e-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
SAMPLE SUMMARY
Client:
Project:
Lab Set ID:
Energy Fuels Resources, Inc.
lst Quarter Surface Water
1303553
Date Received: 3/22/2013 IOIOh
Lab Sample ID Client Sample ID
l303553-001A Cottonwood Creek
1303553-001 A Cottonwood Creek
Date Collected
3/15/2013 l040h
3/15/2013 1040h
Contact: Garrin Palmer
Matrix Analysis
Aqueous Total Dissolved Solids, A2540C
Aqueous TSS
Report Date: 3/2 7/20 13 Page 2 of7
All analyses applicable to the CWA. SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on lhe atlached COC TI1is report is pro\'ided for the exclusi' e use of the addressee Pri,·ileges of
subsequent usc of the name of this company or any member of its staff. or reproduction of this report in connection \\ith Ute ad\'ertisemenL promotion or sale of unr product or process, or in connection \\ith the re-publication of this report for an)
purpose other than for the addressee "111 be granted only on contact This company acceplS no responsibility except for the due performance or inspeclion and/or anal) sis in good fa.ilh and according to the rules of lhe trade and or science
ANA LYTICA L LABORATORIES
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax: [phone]
e-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Inorganic Case Narrative
Client:
Contact:
Energy Fuels Resources, Inc.
Garrin Palmer
Project:
Lab Set ID:
Sample Receipt Information:
Date of Receipt:
Date of Collection:
Sample Condition:
C-0-C Discrepancies:
1st Quarter Surface Water
1303553
3/22/2013
3/15/2013
Intact
None
Holding Time and Preservation Requirements: The analysis and preparation for the
sample was performed within the method holding times. The sample was properly
preserved.
Preparation and Analysis Requirements: The sample was analyzed following the
methods stated on the analytical reports.
Analytical QC Requirements: All instrument calibration and calibration check
requirements were met. All internal standard recoveries met method criterion.
Batch QC Requirements: MB, LCS, RPD, DUP:
Method Blanks (MB): No target analytes were detected above reporting limits,
indicating that the procedure was free from contamination.
Laboratory Control Samples (LCS): All LCS recoveries were within control
limits, indicating that the preparation and analysis were in control.
Duplicate (DUP): The parameters that required a duplicate analysis had RPDs
within the control limits.
Corrective Action: None required.
Report Date: 3/27/2013 Page 3 of7
All anal~ ses applicable to the CWA. SDWA, and RCRA are performed in accordance to NELAC prorocols Pertinent sampling mformation is located on the auached COC This report is prO\ ided for the exclusi\'e use of the addressee Privileges of
subsequent use or the name of this com pan~ or any member of its staff, or reproduction of this report in connection with the ad\·ertisement, promotion or sale of an) product or process, or in connection'' ith the re-pLJblicntion oflhis report for an)
purpose other than for the addressee \\111 be granted. only on contact This company accepts no responsibility excepl for the due perronnance of inspeclion and/or analysis in good faith and <Jccording to lhe rules of the trade and of science
American West "''llltVTtc u 1 A1>0nHonu•
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone]
Toll Free: [phone]
Fax:[phone]
e-mail: [e-mail]
web: www.awal-labs.com
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
INORGANIC ANALYTICAL REPORT
Client:
Project:
Lab Sample ID:
Energy Fuels Resources, Inc.
1st Quarter Surface Water
1303553-001
Client Sample ID: Cottonwood Creek
Collection Date: 3/15/2013 1 040h
Received Date: 3/22/2013 1010h
Analytical Results
Date
Compound Units Prepared
Total Dissolved Solids mg!L
Total Suspended Solids mg/L
Contact: Garrin Palmer
Date Method Reporting
Analyzed Used Limit
3/22/2013 1240h SM2540C 20.0
3/22/2013 1630h SM2540D 3.00
Analytical
Result Qual
436
21.2
Report Date: 3/2 7/20 13 Page 4 of7
All analyses applicable to Lhe CWA_ SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the auached COC This report is prO\ided for the exclusive use of the <1ddressee Pri\ ileges of
subsequent use of lhe name of this compan) or any member of its staff, or reproduction of this repor1 in connectiOn \Hth the ad\ ertisemenL promotion or sale of ID1)1 product or process, or in connect1on \\ ith the re-pubhcation of this report for an)
purpose other Lhan for the addressee \\ill be granted onl) on contact This company accepts no responsibility except for the due perrormance of inspection and/or anal~ sis in good faith and according Lo Lhe rules of the trade and or science
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1303553
Project: lst Quarter Surface Water
SampleiD
1303550-00lCDUP
1303553-00IADUP
1303553-00IADUP
Analyte
Total Dissolved Solids
Total Dissolved Solids
Total Suspended Solids
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
QC SUMMARY REPORT
Contact: Garrin Palmer
Dept: we
QCType: DUP
Amount Original
Units Method Result Spiked Amount %REC Limits
mg!L SM2540C 3,760 3,772 .
mg!L SM2540C 428 436.0
mg!L SM2540D 22 .2 21.20 .
RPD
%RPD Limit
0.319 5
1.85 5
4.61 5
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Qual Date Analyzed
3/22/2013 1240h
3/22/2013 1240h
3/22/2013 1630h
Report Date: 3/27/2013 Page 5 of7
All anaJyses applicable to the CWA, SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC This report is provided for the exclusive use of the addressee Privileges of subsequent use of the name of this company or any
member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact Thls company accepts no responsibility
except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science
American West
ANALYTICAL LABORATORIES
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1303553
Project: lst Quarter Surface Water
Sample ID
LCS-R51899
LCS-R51855
Analyte
Total Dissolved Solids
Total Suspended Solids
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
C SUMMARY REPORT
Contact:
Dept:
Garrin Palmer
we
Units
mg/L
mg!L
Method
SM2540C
SM2540D
Result
186
94.0
Amount
Spiked
205.0
100.0
QCType: LCS
Original
Amount %REC
0
0
90.7
94.0
Limits
80-120
80-120
%RPD
RPD
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Limit Qual Date Analyzed
3/22/2013 1240h
3/22/2013 1630h
Report Date: 3/27/2013 Page 6 of7
All analyses applicable to the CWA. SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC This report is prov1ded for the exclusive use of the addressee Privileges of subsequent use of the name of this company or any
member of its staff, or reproduction of this 1eport in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publ1cation of this report for any purpose other than for the addressee will be granted only on contact This company accepts no responsibility
except for the due performance of inspection and/or analysis in good faith and according to the rules oft he trade and of science
ANALYTICAL
Client: Energy Fuels Resources, Inc.
Lab Set ID: 1303553
Project: 1st Quarter Surface Water
Sample ID Analyte
MB-R51899 Total Dissolved Solids
MB-R51855 Total Suspended Solids
463 West 3600 South
Salt Lake City, UT 84115
Phone: [phone], Toll Free: [phone], Fax: [phone]
e-mail: [e-mail], web: www.awal-labs.com
C SUMMARY REPORT
Contact: Garrin Palmer
Dept: we
QC Type: MBLK
Amount Original
Units Method Result Spiked Amount %REC Limits
mg/L SM2540C < 10.0 -
mg/L SM2540D <3.00 .
RPD
%RPD Limit
Kyle F. Gross
Laboratory Director
Jose Rocha
QA Officer
Qual Date Analyzed
3/22/2013 1240h
3/22/2013 1630h
Report Date: 3/27/2013 Page 7 of7
All analyses applicable to the CWA. SOWA. and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC This report is prov1ded for the exclusive use of the addressee Privileges of subsequent use of the name of this company or any
member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee VIii I be gran led only on contact This company accepts no responsibility
except for the due performance of inspection and/or analysis in good faith and according to the rules of the trade and of science
American West Analytical Laboratories
WORK ORDER Summary a...J
Client: Energy Fuels Resources, Inc. \J s rt
Client ID: DENIOO Contact:
Project: 1st Quarter Surface Water ~ QC Level:
Garrin Palmer
Ill
Conunents: Holding Time Rush. QC 3 EDD-Denison. CC [e-mail];
SampleiD Client Sample ID Collected Date Received Date Test Code
1303553-001A Cottonwood Creek 3/15/2013 1040h 3/22/2013 1010h TDS-W-2540C
TSS-W-2540D
Printed: 3/2212013 FORLABORATORYUSEONLY[filloutonpage1]: %M 0 RT 0 CN 0 TAT 0 QCO HOK __ _
Matrix
Aqueous
HOK __ _
Work Order: 1303553
Due Date: 4/5/2013
WO Type: Standard
Sel Storage
0 ww -tss/tds
0 ww -tss/tds
UL
Denison
Page 1 of 1
HOK___ COC EmaJled.,__ __ _
·Client £.(\c..r.B'/ 1;-ve.l$'
Address 64~5 .St>s.> l:l-. th..>y 1 q l
gt~~ vr Sl_I:{SJI
City Zip State
Phone &.f3S i1V .2 22.\ Fax. ________ __
Contact 6Ad:~:-rl6 P"'-1~~
E-mail 8p-..1..-...v t!?. ~yELJc.lr. LO"'""-
Project Name JSf" ~J.lQ:r-:1:"-:l.: ~~ott::2~.: w..,._t:Sd:
Project Number/P.O.# Date!Time
Sampler Name G ... rt\6 P4.br Collected
Sample 10
c..,++OA. ,..,,.,~ Lr,.L \::. '3/r~lr'l/lo"to
Relinquished By:;;:::;; D J. Date / 3/:u J::S
Received By: Signature
PRINT NAME 64 . O,. \. Time PRINT NAME
~r•..... ......~ • ,.,.,0
Relinquished By: Signature Date Received By: Signature
PRINT NAME Time PRINT NAME
Relinquished By: Signature Date Received By: Slgne(uro
PRINT NAME Time PRINT NAME
Relinquished By: Signature Date Received By: Sigfl8'1Ure
PRINJ: NAME Time PRINT NAME ...
X ·;:: ..... Cll ::2:
AMERICAN
WEST
ANALYTICAL
LABORATORIES
463 West 3600 South
Salt Lake Clty, Utah
84115
CHAIN OF
CUSTODY
[phone]
[phone]
Fax(801)263~7
Email:[e-mail]
TESTS REQUIRED
~ ! ~ !'! ')
I l~ "" ~1 8 ~1 "'. ~ '0
" -:v 1 .c E ~ " ~ ~ z ~
Wl }< ~
/
Date Special Instructions: /
Time .
Date
Time
o~e
Time
Date
Time
Lab Sample Set# f J 0 3 5 f .J
Page of-----
Turn Around Time (Circle One)
1 day 2 day 3 day 4 day 5 day (ijindar"<!:}
.
QC LEVEL LABORATORY USE ONLY
~aE:.
1 2 2+ tes: or hand 1efrverec
~Ex~ ® 3+ 4 2 Amblen OJ' Chilled
Notes:
3 Te!'nperature I 0 r
COMMENTS ·--t!)~ I (Improperly ·
y N
I Notes: .
~·~ _/ y N
I 1!(1 at Bench
N·
I Notes:
I ~-'" J ng Times
I N
0
/
/
I I COC TaJMt Was:
1 Present on Outer
DeN NA
2~n on0uter
Q yu~ M
Y N NA
.f Ul'\bfOken n S~ Y N NA
l:>lscrepand.es Be~ ./ -~,_,.;(j' Record?
y . N,
Notes: •
www.energylab.com EI\ERGY
' ' ;, I I•• Allf1lkfJ ElUIJetf .. 1151
Helena, MT 877-472.0711 • Billings, MT 800-735-4419 • Casper, WY 881-235.0515
Gillatte, WY 11&-116-7175 • Rapid City, SD 118-&72-1225 • College Station, TX 881-610-2211
May 02, 2013
Energy Fuels Resources (USA) Inc
225 Union Blvd Ste 600
Lakewood, CO 80228-1826
Workorder No.: C13040398
ANALYTICAL SUMMARY REPORT
Project Name: 2nd Quarter Surface Water
Energy Laboratories, Inc. Casper WY received the following 2 samples for Energy Fuels Resources (USA) Inc on 4/11/2013
for analysis.
Sample ID Client Sample ID Collect Date Receive Date Matrix Test
C13040398-001 Cottonwood Creek
C13040398-002 Filter Blank
04/10/13 8:15 04/11/13 Surface Water Sample Filtering
Uranium, Dissolved
Uranium, Suspended
Digestion, Total Metals
Gross Alpha minus Rn222 and
Uranium
Radium 226, Dissolved
Radium 226, Suspended
Thorium, Isotopic
Thorium, Suspended Isotopic
Solids, Total Dissolved
Solids, Total Suspended
04/11/13 9:45 04/11/13 Surface Water Sample Filtering
Uranium, Dissolved
Gross Alpha minus Rn222 and
Uranium
Radium 226, Dissolved
Thorium, Isotopic
The results as reported relate only to the item(s) submitted for testing . The analyses presented in this report were
performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted.
Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601,
unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical
Report, the QAIQC Summary Report, or the Case Narrative.
If you have any questions regarding these test results, please call.
Report Approved By:
Digitally signed by
Sheri M. Mead
Date: 2013.05.02 11 :30:17 -06:00
Page 1 of 13
www.energytab.com Helena, MT 871-472-0711 • Billings, MT 8GI-735-44Bfl • Casper, WY 881-235-0515
A-'!fbl Exallwa Sit/a 1/IU
CLIENT: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Surface Water Report Date: 05/02/13
Sample Delivery Group: C13040398 CASE NARRATIVE
RA226 ANALYSIS
USNRC Regulatory Guide 4.14 provides guidance on Minimum Detectable Concentrations (MDC) that should be achieved
in samples for this radionuclide. The sample-specific MDC for this sample could not be achieved due to significant matrix
interferences, restricting the volume of sample to be used in the analysis. Please consult with your local regulatory agency
prior to using these results for compliance purposes.
ORIGINAL SAMPLE SUBMITTAL(S)
All original sample submittals have been returned with the data package.
SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C)
Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are
hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has
begun.
GROSS ALPHA ANALYSIS
Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by
this method for non potable waters should be viewed as inconsistent.
RADON IN AIR ANALYSIS
The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing
should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to
beginning of counting should not exceed 8 days.
SOIUSOLID SAMPLES
All samples reported on an as received basis unless otherwise indicated.
ATRAZINE, SIMAZINE AND PCB ANALYSIS
Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for
seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria
for PCB monitoring.
SUBCONTRACTING ANALYSIS
Subcontracting of sample analyses to an outside laboratory may be required . If so, ENERGY LABORATORIES will utilize
its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the
Laboratory Analytical Report.
BRANCH LABORATORY LOCATIONS
eli-b-Energy Laboratories, Inc. -Billings, MT
eli-g -Energy Laboratories, Inc. -Gillette, WY
eli-h -Energy Laboratories, Inc. -Helena, MT
eli-r-Energy Laboratories, Inc. -Rapid City, SD
eli-cs -Energy Laboratories, Inc . -College Station, TX
CERTIFICATIONS:
USEPA: WY00002, Radiochemical WYD0937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA;
Oregon: WY200001, Radiochemical WY200002; Utah: WYDD002 ; Washington: C836
ISO 17025 DISCLAIMER:
The results of this Analytical Report relate only to the items submitted for analysis.
ENERGY LABORATORIES, INC.-CASPER,WY certifies that certain method selections contained in this report meet
requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered
under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample
state of origin. Please verify Ell's certification coverage by visiting www.energylab.com
Ell appreciates the opportunity to provide you with this analytical service. For additional information and services visit our
web page www.energylab.com.
Page 2 of 13
EI\ERGY
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Helena, MT 817-472-0711 • Billings, MT 801-735-4489 • Casper, WY 881-235-0515
Gillette, WY 81&-188-7175 • Rapid City, SO 188-172-1225 • College Station, 1X 811-610-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Surface Water
Lab ID: C13040398-001
Client Sample ID Cottonwood Creek
Analyses
PHYSICAL PROPERTIES
Solids, Total Dissolved TDS@ 180 C
Solids, Total Suspended TSS@ 105 C
METALS· DISSOLVED
Uranium
METALS-SUSPENDED
Uranium
RADIONUCLIDES-DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
RADIONUCLIDES • SUSPENDED
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
-See Case Narrative regarding Ra226 analysis.
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
Result Units
452 mgll
6 mgll
0.0090 mgll
NO mgll
0.01 pCill
0.3 pCiiL
0.5 pCiiL
0.16 pCiiL
0.12 pCiiL
0.16 pCiiL
-0.01 pCiiL
0.05 pCiiL
0.1 pCiiL
0.37 pCiiL
0.32 pCiiL
0.45 pCiiL
0.1 pCiiL
0.09 pCi!L
0.1 pCiiL
MDC -Minimum detectable concentration
Qualifiers
u
u
u
u
MCL/
RL QCL
10
4
0.0003
0.0003
Report Date: 05/02/13
Collection Date: 04/1 0/13 08:15
Date Received: 04/11/13
Matrix: Surface Water
Method Analysis Date I By
A2540 C 04116113 11:50 I jz
A2540 D 04112/13 10:041 ab
E200.8 04117113 14:32 I cp
E200.8 04117113 17:31 I cp
E900.1 04124113 06:29 llbb
E900.1 04124113 06:2911bb
E900.1 04124113 06:29 I lbb
E903.0 04124113 10:02 I lmc
E903.0 04124113 10:02 I lmc
E903.0 04124113 10:02 I lmc
E908.0 04119113 08:59 I dmf
E908.0 04119113 08:59 I dmf
E908.0 04119113 08:59 I dmf
E903.0 04122/13 16:28 I lmc
E903.0 04122113 16:28 I lmc
E903.0 04122113 16:28 I lmc
E908.0 04118113 16:07 I dmf
E908.0 04118113 16:07 I dmf
E908.0 04118113 16:07 I dmf
MCL-Maximum contaminant level.
NO-Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Page 3 of 13
EN:RGY
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Helena, MT 817-472-0711 • Billings, MT 801-135-4481 • Casper, WY 881-235-0515
Gillstte, 'K'f 818-188-7175 • Rapid City, SO 818-672-1225 • College Station, TX 811-690-2218
LABORATORY ANALYTICAL REPORT
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Surface Water
Lab ID: c 13040398-002
Client Sample ID Filter Blank
Analyses Result Units
METALS-DISSOLVED
Uranium
RADIONUCLIDES-DISSOLVED
Gross Alpha minus Rn & U
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Report
Definitions:
RL-Analyte reporting limit.
QCL-Quality control limit.
NO
-0.1
0.2
0.5
·0.02
0.09
0.16
0.05
0.07
0.1
MDC -Minimum detectable concentration
mg/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCi/L
pCii L
Qualifiers
u
u
u
MCU
RL QCL
0.0003
Report Date: 05/02/13
Collection Date: 04/11/13 09:45
DateReceived: 04/11/13
Matrix: Surface Water
Method Analysis Date I By
E200.8 04/17/13 14:36 / cp
E900.1 04/24/13 06:29/lbb
E900.1 04/24/13 06:29 /lbb
E900.1 04/24/13 06:29 /lbb
E903.0 04/24/13 1 0:02 llmc
E903.0 04/24/13 1 0:02 /lmc
E903.0 04/24/1310:02/lmc
E908.0 04/19113 08:59 I dmf
E908.0 04119113 08:59 I dmf
E908.0 04119/13 08:59 / dmf
MCL -Maximum contaminant level.
NO -Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Page 4 of 13
EN:RGY
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Helena, MT 877-472-0711 • Billings, MT 808-735-4419 • Casper, VNBBI-235-0515
Gillatta, WY 188-888-7175 • Rapid City, SO 118-112·1225 • CoiiBI!e Station, TX 881-610-2218
QAIQC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Surface Water
Analyte Count Result Units
Method: A2540 c
Sample ID: MB-1_130416A Method Blank
Solids, Total Dissolved TDS@ 180 C NO mg/L
Sample ID: LCS-2_130416A Laboratory Control Sample
Solids, Total Dissolved TDS@ 180 C 1970 mg/L
Sample ID: C13040398·001A DUP Sample Duplicate
Solids, Total Dissolved TDS@ 180 C 452 mg/L
Sample ID: C13040401-001A MS Sample Matrix Spike
Solids, Total Dissolved TDS@ 180 C 1450 mg/L
Qualifiers:
RL-Analyte reporting limit.
MDC -Minimum detectable concentration
RL
10
20
10
11
Report Date: 05/02/13
Work Order: C13040398
o/oREC Low Limit High Limit RPD RPDLimlt Qual
Batch: TDS130416A
Run: BAL-19_130416A 04/16/13 11 :49
Run: BAL-19_130416A 04/16/13 11 :50
99 90 110
Run: BAL-19_130416A 04/16/13 11 :50
5
Run: BAL-19_130416A 04/16/13 11 :50
99 90 110
NO-Not detected at the reporting limit.
Page 5 of 13
EN:RGY
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Helena, MT 877-472-8711 • Billings, MT 800-7311·4419 • Casper, WY 811-235-0515
Gillatta, WY 188-186-7175 • Rapid City, SD 818-672-1225 • Collage station, 1X 881-&ID-2211
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Surface Water
Analyte Count Result
Method: A2540 D
Sample ID: MBLK1_130412
Solids, Total Suspended TSS@ 105 C
Method Blank
ND
Units
mg/L
Sample ID: LCS1_130412 Laboratory Control Sample
Solids, Total Suspended TSS @ 1 05 C 199 mg/L
Qualifiers:
RL -Analyte reporting limit.
MDC-Minimum detectable concentration
Report Date: 05/02/13
Work Order: C13040398
RL %REC Low Limit High Limit
Run: BAL-19_130412A
2
Run: BAL-19_130412A
6.0 99 60 110
ND -Not detected at the reporting limit.
RPD RPDLimit Qual
Batch: 130412_1_SLDS-TSS-W
04/12/13 09:28
04/12/13 09:28
Page 6 of 13
EN:RGY
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Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, WY 881-235-0515
Gillette, WV 8&8·&86-7175 • Rapid City, SD 818·&72-1225 • College Station, TX 881-&10-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Surface Water
Report Date: 05/02/13
Work Order: C13040398 ----------------------------------------------------------------------,
Ana lyle Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual
Method: E200.8
Sample ID: ICV
Uranium
Initial Calibration Verification Standard
Analytical Run: ICPMS4-C_130417A
04/17/13 11:10
Sample ID: ICSA
Uranium
Sample ID: ICSAB
Uranium
Method: E200.8
Sample ID: MB-37154
Uranium
Sample ID: LCS-37154
Uranium
Sample ID: C13040470·004AMS
Uranium
Sample ID: C13040470·004AMSD
Uranium
Method: E200.8
Sample ID: C13040389·008BMS4
Uranium
Sample ID: C13040389·008BMSD
Uranium
Qualifiers:
RL-Analyte reporting limit
NO -Not detected at the reporting limit
0.0496 mg/L
Interference Check Sample A
7.00E-05 mg/L
Interference Check Sample AB
1.81E-05 mg/L
Method Blank
5E-05 mg/L
Laboratory Control Sample
0.108 mg/L
Sample Matrix Spike
0.265 pCi/Filter
Sample Matrix Spike Duplicate
0.263 pCi/Filter
Sample Matrix Spike
8.26 mg/L
Sample Matrix Spike Duplicate
8.09 mg/L
0.00030 99 90 110
0.00030
0.00030
Run: ICPMS4-C_130417A
9E-06
Run: ICPMS4-C_130417A
0.00030 108 85 115
Run: ICPMS4-C_130417A
0.00030 106 70 130
Run: ICPMS4-C_130417A
0.00030 105 70 130
Run: ICPMS4-C_130417A
0.00030 70 130
Run: ICPMS4-C_130417A
0.00030 70 130
0.6
2.1
04/17/13 11:15
04/17/13 11:19
Batch: 37154
04/17/13 17:18
04/17/13 17:22
04/17/13 18:15
04/17/13 18:20
20
Batch: R172572
04/17/1314:19
A
04/17/13 14:23
20 A
A-The analyte level was greater than four times the spike level. In
accordance with the method % recovery is not calculated.
MDC -Minimum detectable concentration
Page 7 of 13
EI\ERGY
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Helena, MT 877-472-0711 • Billings, MT BOD-735-4489 • Casper, WY 888-235-0515
Gillatte, WY 8&&-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-&10-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Surface Water
Analyte Count Result Units
Method: E900.1
Sample ID: LCS-GA-0676
Gross Alpha minus Rn & U
Laboratory Control Sample
38.7 pCi/L
Sample ID: MB-GA-0676
Gross Alpha minus Rn & U
3 Method Blank
Gross Alpha minus Rn & U Precision (±)
Gross Alpha minus Rn & U MDC
Sample ID: C13040436-003GMS
Gross Alpha minus Rn & U
Sample ID: C13040436-003GMSD
Gross Alpha minus Rn & U
Qualifiers:
RL-Analyte reporting limit.
MDC-Minimum detectable concentration
-0.3 pCi/L
0.2 pCi/L
0.5 pCi/L
Sample Matrix Spike
84.7 pCi/L
Sample Matrix Spike Duplicate
79.4 pCi/L
Report Date: 05/02/13
Work Order: C13040398
RL %REC Low Limit High Limit RPD RPDLimit Qual
Run: BERTHOLD 770-1_130422A
104 80 120
Run: BERTHOLD 770-1_130422A
Run: BERTHOLD 770-1_130422A
109 70 130
Run: BERTHOLD 770-1_130422A
105 70 130 6.5
ND -Not detected at the reporting limit.
U -Not detected at minimum detectable concentration
Batch: GA-0676
04/24/13 06:29
04/24/13 06:29
u
04/24/13 09:09
04/24/13 10:55
20.4
Page 8 of 13
Er\ERGY
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Helena, MT 877-472-1711 • Billings, MT 800-735-44119 • Casper, WY 8811-235-0515
Gillatta, WY 1166-&BB· 7175 • Rapid City, SO 8118-&72·1225 • College Station, 1X 881-&ID-2218
QAJQC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Surface Water
Analyte Count Result Units
Method: E903.0
Sample ID: C13040398·001AMS
Radium 226
Sample ID: C13040398-001AMSD
Radium 226
Sample ID: MB-37154
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Sample ID: LCS-37154
Radium 226
Method: E903.0
Sample ID: C13040486·001GMS
Radium 226
Sample ID: C13040486·001GMSD
Radium 226
Sample ID: MB-RA226-6600
Radium 226
Radium 226 precision (±)
Radium 226 MDC
Sample ID: LCS·RA226·6600
Radium 226
Qualifiers:
RL-Analyte reporting limit.
Sample Matrix Spike
68 pCi/L
Sample Matrix Spike Duplicate
59 pCi/L
3 Method Blank
-0.1 pCi/Filter
0.1 pCi/Filter
0.3 pCi/Filter
Laboratory Control Sample
21.0 pCi/Filter
Sample Matrix Spike
22 pCi/L
Sample Matrix Spike Duplicate
20 pCi/L
3 Method Blank
-0.03 pCi/L
0.10 pCi/L
0.2 pCi/L
Laboratory Control Sample
11 pCi/L
MDC -Minimum detectable concentration
Report Date: 05/02/13
Work Order: C13040398
RL %REC Low Limit High Limit RPD RPDLimit Qual
Run: BERTHOLD 770-1_130416A
102 70 130
Run: BERTHOLD 770-1 _130416A
89 70 130 14
Run: BERTHOLD 770-1_130416A
Run: BERTHOLD 770-1_130416A
99 80 120
Run: BERTHOLD 770-2_130417A
94 70 130
Run: BERTHOLD 770-2_130417A
88 70 130 6.4
Run: BERTHOLD 770-2_130417A
Run: BERTHOLD 770-2_130417A
97 80 120
ND -Not detected at the reporting limit.
Batch: 37154
04/22/13 16:28
04/22/13 16 :28
21.3
04/22/13 16:28
u
04/22/13 16:28
Batch: RA226-6600
04/24/13 11 :48
04/24/13 11 :48
22
04/24/13 15:48
u
04/24/13 15:48
U-Not detected at minimum detectable concentration
Page 9 of 13
EN:RGY
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Helena, MT 877-472-0711 • Billings, MT BD0-735-4419 • Casper, WY 811-235-0515
Gillette, WY IBB-&86-7175 • Rapid City, SD 888-672-1225 • College Station, TX 881-&ID-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Surface Water
Analyte
Method: E908.0
Sample 10: C13040398-001AMS
Thorium 230
Sample 10: C13040398-001AMSO
Thorium 230
Sample 10: LCS-37154
Thorium 230
Sample 10: MB-37154
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Method: E908.0
Sample 10: LCS-RA-TH-IS0-1826
Thorium 230
Sample 10: C13040398-002AMS
Thorium 230
Sample 10: C13040398-002AMSO
Thorium 230
Sample 10: MB-RA-TH-IS0-1826
Thorium 230
Thorium 230 precision (±)
Thorium 230 MDC
Qualifiers:
RL-Analyte reporting limit.
Count Result Units
Sample Matrix Spike
35 pCi/L
Sample Matrix Spike Duplicate
34 pCi/L
Laboratory Control Sample
16.0 pCi/Filter
3 Method Blank
3
0.02 pCi/Filter
0.09 pCi!Filter
0.2 pCi/Filter
Laboratory Control Sample
5.8 pCi/L
Sample Matrix Spike
12 pCiiL
Sample Matrix Spike Duplicate
10 pCi/L
Method Blank
0.4 pCi/L
0.2 pCi/L
0.2 pCi!L
MDC -Minimum detectable concentration
Report Date: 05/02/13
Work Order: C13040398
RL %REC Low Limit High Limit RPO RPOLimit Qual
Batch: 37154
Run: ALPHANAL YST _130416A 04/18/13 16:07
115 70 130
Run: ALPHANAL YST_130416A
110 70 130 4.9
04/18/13 16:07
31
Run: ALPHANAL YST_130416A
104 80 120
Run: ALPHANAL YST_130416A
Run: EGG-ORTEC_130416A
92 80 120
Run: EGG-ORTEC_130416A
98 70 130
Run: EGG-ORTEC_130416A
84 70 130
Run: EGG-ORTEC_130416A
ND -Not detected at the reporting limit.
04/18/13 16:08
04/18/13 16:08
u
Batch: RA-TH-IS0-1826
04/19/13 08:59
17
04/19/13 08:59
04/19/13 08:59
39.4
04/19/13 13:54
U -Not detected at minimum detectable concentration
Page 10 of 13
EN:RGY
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Halena, MT 817-472-0711 • Billints. MT BOD-735-4419 • Casper, WY 881-235-0515
Gillatta, WY 116·188-7175 • Rapid City, SD IIB-172·1225 • Colleae Station, 1X 881-610-2218
QA/QC Summary Report
Prepared by Casper, WY Branch
Client: Energy Fuels Resources (USA) Inc
Project: 2nd Quarter Surface Water
Analyte Count Result Units
Method: SW6020
Sample ID: C13040470-004AMS
Uranium
Sample 10: C13040470-004AMSD
Uranium
Sample ID: MB-37154
Uranium
Sample ID: LCS-37154
Uranium
Sample 10: C13040398-001ADIL
Uranium
Qualifiers:
RL-Analyte reporting limit.
MDC -Minimum detectable concentration
Sample Matrix Spike
0.252 mg/filter
Sample Matrix Spike Duplicate
0.250 mg/filter
Method Blank
5E-05 mg/filter
Laboratory Control Sample
0.108 mg/filter
Serial Dilution
0.000189 mg/filter
Report Date: 05/02/13
Work Order: C13040398
RL %REC Low Limit High Limit
Run: ICPMS4-C_130417A
0.00030 101 75 125
Run: ICPMS4-C_130417A
0.00030 100 75 125
Run: ICPMS4-C_130417A
9E-06
Run: ICPMS4-C_130417A
0.00030 108 85 115
Run: ICPMS4-C_130417A
0.00030
NO -Not detected at the reporting limit.
RPD RPDLimit Qual
0.6
Batch: 37154
04/17/13 18:15
04/17/13 18:20
20
04/17/13 17:18
04/17/13 17:22
04/17/13 17:36
20 N
N -The analyte concentration was not sufficiently high to calculate a
RPD for the serial dilution test.
Page 11 of 13
EN:RGY
., '
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~fJUAfocllsece tm Helena, fliT 877-472-11711 • Billings, MT 801·735-4489 • Casper, WY 888-235-1515
Gillatta, WY 811-111-7175 • Rapid City, SD 1188-172-1225 • College Station, TX 8118-&ID-22111
Standard Reporting Procedures
Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual
Chlorine, are qualified as being analyzed outside of recommended holding time.
Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry.
For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis.
Workorder Receipt Checklist
Energy Fuels Resources (USA) Inc
Login completed by : Kerri Schroeder
Reviewed by: BL2000\kmiller
Reviewed Date: 4/12/2013
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
(Exclude analyses that are considered field parameters
such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.)
Temp Blank received?
Container/Temp Blank temperature:
Water • VOA vials have zero headspace?
Water · pH acceptable upon receipt?
Yes 0
Yes 0
Yes D
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes 0
Yes D
4. 6 "C On Ice
Yes D
Yes 0
C13040398
Date Received: 4/11/2013
Received by: ks
NoD
NoD
NoD
NoD
No 0
NoD
NoD
NoD
NoD
NoD
NoD
No 0
Carrier NDA
name:
Not Present D
Not Present D
Not Present 0
Not Applicable O
No VOA vials submitted 0
Not Applicable O
-----------------------------------------------------------------
Contact and Corrective Action Comments:
Sample was filtered and preserved in the laboratory for dissolved and suspended analyses.
Page12of13
Sheet 1 of 1
CHAIN OF CUSTODY
Samples Shipped to: -:E:'::n~e~rgy~L~a.;.;;;b~s-__,. ______ Contact:
2393 Salt Creek Hwy
Garrln Palmer
Ph: 435 678 2221
Casper, WY 82601 gpalmer.@ energytue!s.com
nholl!day@ eqergytuels.oom
dturk@ energytuels.com
Chain of Custody/Sampling Analysis Request
Project Samplers Name sam~ers S!g_nature
2nd Quarter Surface &-~ ?~ Water 2013 Garrin Palmer
Date Time
Sample ID Collected Collected Laboratory Ana!Y_sls Requested
Cottonwood Creek 4/10/201'3 815 TDS
TSS
Gross Alpha
Syspended/Dissolved U-NAT
Suspended/Dissolved Ra 226
Suspended/Dissolved TH-230
•samples are non filtered and non preserved
Please notify Garrin PaJmer or Tanner Holliday of Reclept tempature on these samples Immediately!
Thank you.
Relinquished By:(Signature)
? ,._::;;;-~
Relinquished By:(Signature)
Oatemme
Cl3~~()p'!!
~s'Nj~ftJPa~13
White Mesa Mill -Standard Operating Procedures
Book #I 1: Environmental Protection Manual, Section 2.1
Date: 2/07 Revision: DUSA-l
Page 5 of5
Attachment A
FIELD WATER ANALYSIS SURFACE WATER
WHITE MESA MILL
LOCATION (Circle ~ Westwater Canyon Other (describe) ___ _
DATE: :/15/2.0(3> BY: &o..rr•~ P~lwt-c:r ---=----------~----(Sampler's initials)
pH BUFFER 7.0 __ 7_. _0 __ _ pH BUFFER 4.0 _ ___,!..{-'-, ..::.0 ____ _
SPECIFIC CONDUCTIVITY -~G',._' _.q....:.Cl ..... 1 _______ __.u=·MH=· =O=s
STEAM DEPTH:
pHofWATER __ -~7~··c~tg~-------
COND umhos 65~.3
pH Units _'7"'--._.'1 ..... &:...._ __ _
Temp oc __..;,..!>$'-. _U __ _
COND ~-tmhos £55
pH units __ <f=--·_.J~[L. __
Temp °C __ 8"---'. /'-2-__ __
Comments:
TEMP $~I :J-
COND ~-tmhos b54
pHunits 1.q~
Temp°C i).['~
COND j.tmhos ~ S7
. '
pH units __ 7_,__• q-"-'='~'----­
Temp °C _ _:6,_ . ...:-J 2._-=----
I
S.o.~plcs pe..r{;rncdt
..
White Mesa Mill -Standard Operating Procedures
Book# 11: Environmental Protection Manual, Section 2.1
Date: 2/07 Revision: DUSA-1
PageS of5
Attachment A
FIELD WATER ANALYSIS SURFACE WATER
WHITE MESA MILL
LOCATION (Circle one):CottonwoOd Creek dfestwarer CanY§ibOther (describe) ____ _
DATE:_'-+-/_.__! <~l--'-1-"'-~---
pH BUFFER 7.0 __ 7-<--=... =C'-... , __
BY: 1{ e~n· \ ,--.._ ~")~ { .............. ~~
(Sampler's initials)
pH BUFFER 4.0 __ L-......,/..'-'-("'-) __ _
SPECIFIC CONDUCTIVITY _ ___t_1_,Cf_4.___ _____ 1l=M=H=O=s
STEAM DEPTH:
pH of WATER __________ _ TEMP ______ _
'I
COND ;:::1-m=lh=os,__ ___ _ COND~~mh==os"-------
pH Units ______ _ pH units ______ _
Temp °C -------Temp °C ______ _
COND ~mh==os,__ ___ __ COND~mh==os"-------
pH units -------pH units -------
Temp°C ______ _ Temp °C -------
Comments:
s:·~~ . .M
·.
~ •' :·
White Mesa Mill -Standard Operating Procedures
Book #11: Environmental Protection Manual, Section 2.1
Date: 2/07 Revision: DUSA-1
Page 5 of 5
Attachment A
FIELD WATER ANALYSIS SURF ACE WATER
WHITE MESA MILL
Westwatet Can on Other (describe) ____ _
DATE: Lj I :.2/ i3
pH BUFFER 7.0 __ 7"'--' . ._.L..c...'/ __ _
BY: Gc.-rrj,.,._ Pc...L ..... y,r
(Sampler's initials)
pH BUFFER 4.0 _ _:Y:u.•j.,!O~---
SPECIFIC CONDUCTIVITY __ q~'i-+'f------=uMH==O'""'s
STEAM DEPTH: 3 H --~~---------
pHofWATER ________ ~-7~.~7-:7~-----
C.o .... J.
COND umhos 70 .3
pHUnits 7 72
COND ltmhos 7 0 L.j
pH units --7-J...A-• -J7'-7.s---
Temp °C -~.5~~ _.y_,., __ _
Comments:
TENW ______ ~E~-~~~9~
COND f.Lmhos 7() 5'
pH units 7. ~ z
Temp°C 5.So
COND ltmhos 7Q/)
pH units 7 -7 9
Temp °C 5. Y B'
• I
White Mesa Mill -Standard Operating Procedures
Book #11: Environmental Protection Manual, Section 2.1
Date: 2/07 Revision: DUSA-1
Page 5 of 5
Attachment A
FIELD WATER ANALYSIS SURFACE WATER
WHITE MESA MILL
LOCATION (Circle one):Cottonwood Creek QXiitwater Can~ Other (describe) ____ _
DATE: Y /2./1 3
pH BUFFER 7.0 __ 7~~u.""----
BY: .?.<;,. r .-j !A Y 6..-l )e:!A e.c
(Sampler's initials)
pH BUFFER 4.0 __ 1-l..!...:-:....::o::...__ __ _
SPECIFIC CONDUCTIVITY _ ...... 9 ...... '1_..'t ______ -=gMH==O=s
STEAM DEPTH:
pHofWATER ___________ _ TEMP ______ _
• I
COND ~umh=,o><-s ____ _ COND~mh~o~s~-----
pH Units ______ _ pH units ______ _
Temp °C ______ _ Temp °C ______ _
COND ~=mh=os=------COND ~.~mh=os~----
pH units ______ _ pH units ______ _
Temp °C -------Temp °C -------
Comments:
5 /'1{ i3 Arr·'j.,;e c.l 0" s\Jo!.. fA.+ ltJe>o. Gc.,rr)A. ('tt 51'.-A-+1 l rc.e .. [. LYe..\" eJ..~t• .Su fL..,fa,
6/:L6/13 .Arl-;..,e..J.. (}A.. site. ~{. l ;Loo_ Gc~r,..;ol\. .1 Do..v·.cA. fJn .. SC.A t \ G.rc:..:. t wc...s dvr-y . J.'.:..c_ p \...c 1-o.
0
Q
0
--
ATTACHMENT I
SOTI.. SAMPLE GRAPHS, DATA TABLE, LABORATORY RESULTS AND QA!QC
Soil samples are collected during the third quarter. This attachment has been deliberately left
blank.