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HomeMy WebLinkAboutDRC-2013-001421 - 0901a0688035345fENERGYFUELS Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www.energyfuels.com February 27,2013 VIA OVERNIGHT DELIVERY Mr. Rusty Lundberg Director of the Utah Division of Radiation Control State of Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144850 Sah Lake City, UT 84116-4850 Dear Mr. Lundberg: DRC-20 Re: State of Utah Radioactive Material License No. UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period July 1,2012 through December 31,2012 As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65 (subpartl)), and License Condition 11.3A of State of Utah Radioactive Materials License No. UTl900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill for the period July 1, 2012 through December 31, 2012. If you have any questions regarding this report, please contact the undersigned at (303) 389- 4132. Yours very truly. ENERGY FUELS RESOURCES (USA) INC. Jo Ann Tischler Manager, Compliance and Licensing cc: David C. Frydenlund Harold R. Roberts David E. Turk Katherine A. Weinel Central Files February 27,2013 VIA OVERNIGHT DELIVERY Mr. Rusty Lundberg Director of the Utah Division of Radiation Control State of Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144850 Salt Lake City, UT 84116-4850 Dear Mr. Lundberg: Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 3039742140 www.energyfuels.com Re: State of Utah Radioactive Material License No. UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period July 1, 2012 through December 31, 2012 As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65 (subpart 1 )), and License Condition 11.3A of State of Utah Radioactive Materials License No. UT1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill for the period July 1,2012 through December 31, 2012. If you have any questions regarding this report, please contact the undersigned at (303) 389- 4132. Yours very truly, ~~ ENERGY FUELS RESOURCES (USA) INC. JoAnn Tischler Manager, Compliance and Licensing cc: David C. Frydenlund Harold R. Roberts David E. Turk Katherine A. Weinel Central Files White Mesa Uranium Mill Radioactive Materials License UT900479 Semi-Annual Effluent Monitoring Report (July through December 2012) Prepared For: Utah Department of Environmental Quality Division of Radiation Control Prepared by: Energy Fuels Resources (USA) Inc. 225 Union Boulevard, Suite 600 Lakewood, CO 80228 February 27, 2013 Table of Contents 1.0 INTRODUCTION .................................................................................................. 1 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING ..................................... 2 2.1 Program Overview ............................................................................................... 2 2.2 Sampling Protocol and Analytical Results ........................................................... 2 2.3 General Observations ........................................................................................... 3 2.4 Site Specific Sampling Data ................................................................................. 4 2.5 Radon-222 ............................................................................................................ 6 3.0 EXTERNAL RADIATION (DIRECT GAMMA) .................................................. 7 4.0 VEGETATION SAMPLES ..................................................................................... 8 5.0 STACK SAMPLING ............................................................................................... 9 6.0 SURFACE WATER MONITORING .................................................................... 11 7.0 SOIL SAMPLING ................................................................................................. 11 8.0 METEOROLOGICAL MONITORING ................................................................ 11 9.0 SIGNATURE ......................................................................................................... 12 LIST OF TABLES Table 1 NCRP Report 94-Global Pb-21 0 Concentration Example Table 2 Air Monitoring Station Results U-Nat (Comparison to Limits) Table 3 Air Monitoring Station Results Th-230 (Comparison to Limits) Table 4 Air Monitoring Station Results Ra-226 (Comparison to Limits) Table 5 Air Monitoring Station Results Pb-210 (Comparison to Limits) Table 6 Environmental OSL Dosimeter Measurements (Gamma) Table 7 Stack Sampling Requirements Table 8 Stack Effluent Concentrations and Release Rates 1 INDEX OF TABS A High Volume Air Monitoring Stations B BHV Air Sampling Graphs and Data Tables Tab 1 BHV -1 Air Sampling Graphs and Data Table Tab 2 BHV-2 Air Sampling Graphs and Data Table Tab 3 BHV-3 Air Sampling Graphs and Data Table Tab 4 BHV-4 Air Sampling Graphs and Data Table Tab 5 BHV -5 Air Sampling Graphs and Data Table Tab 6 BHV-6 Air Sampling Graphs and Data Table C BHV Air Sampling Laboratory Results and QAlQC D Air Particulate Loading Graphs and Supporting Data E Environmental Gamma (OSL) Dosimeter Graphs and Supporting Data F Vegetation Graphs, Data Table, Laboratory Results and QAlQC G Stack Sample Laboratory Results H Surface Water Graphs and Field Data Sheets I Soil Sample Graphs, Data Table, Laboratory Results and QAlQC ii WHITE MESA URANIUM MILL SEMI-ANNUAL EFFLUENT REPORT, JULY THROUGH DECEMBER 2012 1.0 INTRODUCTION The White Mesa Mill (the "Mill") has established monitoring programs to evaluate compliance with effluent limitations and to assess the potential for release of radioactive material into the local environment. These monitoring programs were developed and implemented at the time of Mill construction, operated with appropriate adaptation over time, and are consistent with the Mill's State of Utah Radioactive Materials License No. UT1900479 (the "License") and guidelines developed by the United States Nuclear Regulatory Commission ("NRC") (NRC Regulatory Guide 4.14, Radiological Ejjluent and Environmental Monitoring at Uranium Mills-Rev. 1, ML003739941), 1980). Under these programs, the Mill monitors the following environmental media and conditions: a) Airborne particulate radionuclide concentrations obtained from the following sampling stations: • North, east and south of the Mill Site: BHV-1 and BHV-2 (north), BHV-5 (east), and BHV-4 (south). BHV-1 serves as a surrogate for the nearest resident (BHV -1 is approximately 1.2 miles north of the Mill, but approximately 0.4 miles closer to the Mill than the nearest resident); • A background location distant to and west of the Mill (BHV-3), which was monitored for airborne particulate up until November, 1995, at which time background was established, but is no longer monitored for air particulate; and • A station specifically requested by the White Mesa Ute Community south of the Mill Site (BVH-6); b) External (direct) gamma radiation measured at air monitoring stations BHV -1, BHV-2, BHV-3, BHV-4, BHV-5 and BHV-6; c) Vegetation at three site periphery locations, for uptake of radiation; d) Stack release rates from the Mill's air emissions sources; e) Surface water at Cottonwood Creek and, when flowing, Westwater Creek, both located west of the Mill; f) Soil radionuclide activity obtained near the air particulate monitoring stations, during the third quarter of each year; 1 N:\WMM\Required Reports\Semi Annual Effluent Reports\2012 July -Dec\JuILtoDec_2012_SAER_text.docx g) Groundwater (up and down gradient) of the Mill facility; andl h) Seeps and springs in the vicinity of the Mill.l This semi-annual effluent report provides the results of the specific monitoring and sampling activities that were undertaken during the subject reporting period. 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING 2.1 Program Overview The environmental airborne particulate monitoring program at the Mill utilizes four air sampling stations. Four high-volume continuous air sampling stations (BHV-l, BHV-2, BHV -4, and BHV -5) are required by the License. These sampling stations serve as sentinels for airborne particulate which could potentially emanate from the Mill site. In addition to its general site monitoring function, BHV -1 also serves as a conservative surrogate for concentrations at the nearest resident, because it is located approximately 1.2 miles north of the Mill just south of the nearest resident but between the Mill and that resident. With regard to background monitoring, the Mill previously operated a continuous high- volume air sampling station (BHV-3) which was located approximately 3.5 miles west of the Mill site. With the approval of NRC, this station (BHV-3) was removed from the active air monitoring program in November 1995. At that time, NRC determined that a sufficient air monitoring data base had been compiled at BHV-3 to establish a representative airborne radionuclide background for the Mill. It should be noted, however, that while air sampling was discontinued at this location, gamma measurements and soil sampling continue at BHV-3. In addition to the environmental air sampling locations described above, an additional station (BHV -6) was installed at the request of the White Mesa Ute Community. This station began operation in July of 1999 and provides airborne particulate information in the southerly direction between the Mill and the White Mesa Ute Community. 2.2 Sampling Protocol and Analytical Results Airborne particulate monitors are operated continuously at each of the high-volume air sampling stations referenced above except BHV -3, as noted above. Particulate sample collection filters are gathered by site technicians weekly in accordance with the Mill's environmental air sampling procedures and are compo sited on a quarterly basis for laboratory analyses. The collected filters are analyzed for Unat activity, Th-230 activity, Ra-226 activity, and Pb-210 activity. Fugitive dust standards for the facility are limited by the Mill's State of Utah Air Approval Order, which sets a 20% visual opacity 1 Groundwater sampling and seeps and springs sampling are reported separately pursuant to the Mill's State of Utah Ground Water Discharge Permit No. UGW370004, and are not included with this report. 2 N:\WMM\Required Reports\Semi Annual Effluent Reports\20l2 July -Dec\JuILtoDec_20l2_SAER_text.docx standard. The specific locations of the Mill's airborne particulate monitoring stations are depicted on the figure entitled High V olume Air Monitoring Stations included as Attachment A. Station BHV-3, which is no longer sampled for air particulate, is located approximately 3.5 miles west of the Mill facility and is not indicated on that Figure. The analytical results of radionuclide particulate sampling for each monitoring station operated during this reporting period are provided in Attachment B under separate sampling station attachment tabs (Tabs 1-6). Each Tab contains graphical illustrations of the radionuclide concentrations in log-scale presentation format. The graphs display reported data over time since the 1981 inception of the Mill's environmental air particulate monitoring program. The actual analytical results (and associated QAlQC information) reported by the laboratory for the reporting period are provided under Attachment C. In addition to the analyses for radionuclides, particulate loading is determined for each filter and compo sited as a quarterly mass-loading estimate for review purposes only. Graphs showing particulate loading at each station and the underlying data are included as Attachment D. It should be noted that for BHV -6 the first 2 sampling periods of April 2012 have been omitted from particulate loading on the graph in Attachment D. The timer on the airborne particulate monitoring station at BHV -6 malfunctioned, and the data are considered invalid due to the inability to measure the time sampled. The timer was replaced prior to the third sampling period and all other measurements are valid. It should be noted that for graphical illustration purposes, values reported at zero, values reported at less than the prescribed detection limit « 1 x 10-16 uCilml) and missing values were plotted as 1 x 10-16 uCi/ml concentrations. Where other "less than" values were indicated (Le., where detection limits for the data varied from 1 x 10-16 uCi/ml), the detection limit concentration was utilized for plotting the data point. This graphing convention is not utilized to formulate station average information, nor is it intended as a precedent for data treatment. Rather, the intent is to provide a conservative viewable depiction of site airborne radionuclide information. This is considered to be a conservative approach because the actual concentration below the detection limit cannot be determined and, as a result, the plotted point will be at the same or a higher concentration than the actual activity concentration of the collected sample. 2.3 General Observations The results of environmental air monitoring for this semi-annual period indicate that for all radionuclides at all monitoring stations airborne radionuclide particulate activity concentrations were well below regulatory Effluent Concentration Limits ("ECL' s") and the Mill's ALARA goals, which are set at 25% of the ECLs. It is noteworthy and expected that Pb-210 concentrations are elevated when compared to the other parent radionuclide concentrations (i.e. V-nat, Th-230 and Ra-226). This phenomenon is due to the well-established controlling effect experienced worldwide as a 3 N:\WMM\Required Reports\Semi Annual Effluent Reports\2012 July -Dec\July_toDec_2012_SAER_text.docx result of the ubiquitous presence of radon in the earth's atmosphere. Accordingly, elevated Pb-210 presence in disequilibrium with parent radionuclides measured here is not associated with uranium milling operations. Rn-222 emanates as a decay-chain progeny of the Ra-226 contained in the soil of the earth's crust and is dispersed generally throughout the earth's atmosphere. The electrically charged short and long-lived decay products of Rn-222 attach to ambient dust particles found naturally in the atmosphere and are carried with the air. Pb-210 is the longest lived of these decay products and is the decay product of the shorter-lived radon progeny. As such, it accumulates as an electrical attachment on the natural ambient dust in the atmosphere and is generally measured at elevated activity when compared to local decay-chain parent radionuclide activity, regardless of uranium milling activity. At the Mill's BHV air monitoring stations, all dust (ambient natural and mill derived) is collected by the sample filter. Because of the natural elevation of Pb-210 accumulated as an attachment to the naturally occurring ambient dust particles collected by the air sampling equipment, Pb-210 is commonly elevated and in disequilibrium when compared to parent radionuclide activity, regardless of the Mill's presence. By way of illustration, average ground-level concentrations have been reported for selected States (NCRP Report 94, 1992) and are summarized in Table 1 below, demonstrating elevated Pb-210 activity where no uranium milling operations are located nearby. Pb-210 activity concentrations can be expected to be even higher for locations in the western u.S. where uranium ore bodies are commonly located. In April 1977, prior to Mill construction and Mill operations, air particulate Pb-21 0 was measured at the Mill site to be 1.3E-14 uCi/ml (13.0E-3 pCi/m3i Table 1-NCRP Report 94-Global Pb-210 Concentration Example 2.4 Site Specific Sampling Data The results of airborne particulate monitoring for the period (without background subtraction) are provided by sampling station and radionuclide in Tables 2 through 5 below. Along with these data, the tables present comparative ECL's and the ECL percentage measured at each of the monitoring stations sampled during the period. A review of these data supports the conclusion that airborne particulate is well controlled at the Mill. In all cases, the measured activity concentrations were well within the ECL, as well as the Mill's ALARA goal (i.e. 25% of the ECL). Lower Limits of Detection 2 See the Environmental Report, White Mesa Uranium Project, San Juan County, Utah for Energy Fuels Nuclear, Inc. prepared by Dames & Moore, January 30, 1978, Section 2.9.1.1 4 N:\WMM\Required Reports\Semi Annual Effluent Reports\2012 July -Dec\July_toDec_2012_SAER_text.docx consistent with NRC Regulatory Guide 4.14 were maintained by the Mill's contract analytical laboratory for this reporting period. In fact, the data obtained since program inception in 1981 indicates that only one individual quarterly measurement (Th-230 at BHV -5 for the 2nd Quarter of 1996) has ever exceeded the ECL at the Mill. With regard to that particular single measurement, while it is important to consider and evaluate an individual measurement exceeding the ECL, for public dose estimation purposes, it is the average annual concentration that is of primary significance. In that instance, the average annual concentration of Th-230 for BHV-5 in 1996 was well below the ECL. Data obtained since program inception in 1981 also indicate that, with very few exceptions, the gross (background inclusive) measurements do not exceed the site's ALARA goal (i.e. only nine of the several thousand total gross radionuclide determinations to date exceeded the Mill's self-imposed 25% ALARA goal). Table 2-Air Monitoring Station Results U-Nat (Comparison to Limits) 3rd and 4th Quarters 2012 Table 3-Air Monitoring Station Results Th-230 (Comparison to Limits) 3rd and 4th Quarters 2012 5 N:\WMM\Required Reports\Semi Annual Effluent Reports\2012 July -Dec\July_toDec_2012_SAER_text.docx Table 4-Air Monitoring Station Results Ra-226 (Comparison to Limits) 3rd and 4th Quarters 2012 Table 5-Air Monitoring Station Results Pb-210 (Comparison to Limits) 3rd and 4th Quarters 2012 2.5 Radon-222 Due to the unavailability of monitoring equipment to detect the revised 10 CFR Part 20 standard, and with the approval of NRC, Radon 222 monitoring at BHV stations was discontinued in 1995. Instead, compliance with these limits and the requirements of R313-15-301 is demonstrated by a calculation, authorized by the NRC and as contemplated by R313-15-302(2)(a). A copy of the Technical Evaluation Report evidencing such approval was enclosed with correspondence to the Division of Radiation Control ("DRC") on July 28, 2008. This calculation is performed by use of the MILDOS code for estimating environmental radiation doses for uranium recovery operations (Strenge and Bender 1981) and more recently in 2003 by use of the updated MILDOS AREA code (Argonne 1998). The analysis under both the MILDOS and MILDOS AREA codes assumes the Mill to be processing high grade Arizona Strip ores at full capacity, and calculates the concentrations of radioactive dust and radon at individual receptor locations around the Mill. 6 N:\WMM\Required Reports\Semi Annual Effluent Reports\2012 July -Dec\July_toDec_2012_SAER_text.docx The MILDOS and MILDOS AREA codes calculate the combined Total Effective Dose Equivalent ("TEDE") from all relevant pathways, including both air particulate and radon, at a number of locations including the nearest residence (the individual likely to receive the highest dose from the licensed operation), approximately 1.6 miles north of the Mill. These calculations reveal projected doses to the individual likely to receive the highest dose from the licensed operations to be well below the 1 00 mrem regulatory limit in R313-15-301(1)(a) for all pathways, including air particulate and radon, and well below the ALARA goal of 10 mrem/yr for air emissions excluding radon as set out in R313-15-101(4). MILDOS AREA modeling was recently conducted in support of the Mill's 2007 License Renewal Application, utilizing the MILDOS-AREA code (Version 2.20~), to estimate the dose commitments at various receptor locations for processing of Colorado Plateau ore (0.25% U308 and 1.5% V20 5) and Arizona Strip ore (0.637% U308). The process rate was assumed to be at full capacity of 730,000 tons per year (an average of 2,000 tons per day) with an average uranium recovery yield of 94%. That modeling showed a TEDE of2 mrem per year at the nearest resident (3 mrem per year at the nearest potential residence, being the location of BHV -1 at the northern property boundary of the Mill site), which included the dose from all radionuclide sources, including radon. The modeled dose from radon itself was therefore a fraction of TEDE and well within the regulatory limits. 3.0 EXTERNAL RADIATION (DIRECT GAMMA) Gamma exposure rate estimates were measured for the reporting period utilizing passive integrating devices, optically stimulated luminescence dosimeters ("OSLs"). These dosimeters were located at each of the Mill's high-volume air sampling stations (BHV-l, BHV -2, BHV -4, BHV -5 and BHV -6) and at the designated background monitoring station (BHV -3). Measurements obtained from location BHV -3 have been designated as background due to BHV-3's remoteness from the Mill site (i.e. BHV-3 is located approximately 3.5 miles west of the Mill site). The results of the environmental OSL measurements and semi-annual cumulative above-background data are provided in Table 6 below. In addition, measurement data obtained at these locations are graphically presented at Attachment E to this report. 7 N:\WMM\Required Reports\Semi Annual Effluent Reports\2012 July -Dec\July_toDec_2012_SAER_text.docx Table 6-Environmental Optically Stimulated Luminescence Dosimeter Measurements (Gamma) *N egative values treated as zero for cumulative dose The results for this period indicate that above background measurements for stations BHV -1, BHV -2, BHV -4, BHV -5 and BHV -6 are within regulatory limits. BHV -1 is at the location of the nearest potential residence. The nearest actual residence is approximately 0.4 miles north of BHV-l. The annual individual member of the public limit is 100 mremlyr for combined internal and external exposure. 4.0 VEGETATION SAMPLES Vegetation samples are collected at three locations around the Mill property. The sampling locations are: 1) northeast, 2) northwest and 3) southwest of the Mill facility. The U.S. Nuclear Regulatory Commission ("NRC") Regulatory Guide 4.14 requires that three samples be collected during the grazing season, without specifying exact months or times during the season. During the 2012 grazing season, three sets of samples were collected on April 11, 2012, June 11, 2012, and November 6, 2012. The data from the April and June sampling were included in the January through June 2012 Semi-Annual Effluent Report ("SAER") which was submitted to the DRC on August 22, 2012. Data from the November sampling event are included in this report. Graphical log-scale presentation of the vegetation sampling results, together with the analytical results reported by the Mill's contract laboratory (including QAlQC information) for this sampling period, are included at Attachment F of this report. The 2012 data results are within the variation of previous sampling episodes. 8 N:\WMM\Required Reports\Semi Annual Effluent Reports\2012 July -Dec\July_toDec_2012_SAER_text.docx 5.0 STACK SAMPLING Under Section 5.0 of Tab 1.4 of the Mill's Environmental Protection Manual, Revision: EFR-3, 12/12 (the "Environmental Protection Manual") gas stack samples are collected at the Mill in accordance with the calendar year schedule shown below: Table 7 -Stack Sampling Requirements Frequency Feed Stack (Grizzly Stack for Packaging Baghouse) Yellowcake Dryer (Yellowcake Baghouse) Quarterly None If operating, U -nat If operating, U -nat Semi-annually If operating, U-nat, If operating, U -nat, If operating, U-nat, Th-23 0 Th-230, Ra-226, Pb-Th-230, Ra-226, 210 Pb-210 The north yellowcake dryer and yellowcake baghouse operated during the 3rd quarter of 2012. The south yellowcake dryer, yellowcake baghouse, and grizzly baghouse operated during the 4th quarter of2012. The analytical results of stack sampling conducted for the 1 st and 2nd quarters of 2012, as well as for the 3rd and 4th quarters of 2012, are provided in Table 8 below, indicating the uCi/cc concentration in the stack emissions and the stack's radionuclide release rate (uCi/sec) for U-Nat, Th-230, Ra-226 and Pb-210 at each of the stacks sampled. The actual analytical results reported by the laboratory for the 3rd and 4th quarters of 2012 are provided in Attachment G to this report. It is also important to note that stack effluent concentrations are not comparable to environmental air sampling station ECL' s for regulatory compliance purposes. The ECL is a limit that applies to the receptor locations and is not applicable to effluents from mill processes on the Mill site. These stack release data are more appropriately utilized for dose modeling purposes, and dose modeling is not computed for semi -annual reporting purposes. 9 N:\WMM\Required Reports\Semi Annual Effluent Reports\2012 July -Dec\July_toDec_2012_SAER_text.docx Dryer, Run 1 North YC Dryer, Run 2 North YC Dryer, Run 1 North YC Dryer, Run 2 Yellowcake Baghouse Dryer, Run 1 North YC Dryer, Run 2 Yellowcake South YC Dryer, Run 1 South YC Dryer, Run 2 Yellowcake Baghouse Grizzly Baghouse Table 8-Stack Effluent Concentrations and Release Rates 9.71E-09 5.59E-03 1.27E-08 7.53E-03 6.33E-I0 1. 12E-08 5.60E-03 1.54E-13 7.72E-08 1.37E-14 6.84E-09 3.25E-12 1.63E-06 1. 13E-08 6.75E-03 2.45E-12 1.47E-06 2.13E-14 1.28E-08 2.27E-12 1.36E-06 3.04E-09 3.32E-03 1. 15E-11 1.25E-05 7.80E-14 8.50E-08 3.64E-13 3.97E-07 *Not *Not 8.46E-09 5.51E-03 6.56E-09 4.49E-03 1. 19E-09 1.71E-03 1.28E-09 1.19E-03 2.46E-13 2.29E-07 1.44E-14 1.35E-08 4.15E-13 3.88E-07 6.28E-I0 6.08E-04 2.07E-13 2.00E-07 1.05E-14 1.01E-08 3.53E-13 3.42E-07 2.93E-09 4.81E-03 1.60E-12 2.62E-06 4.52E-14 7.43E-08 5.01E-13 8.24E-07 2.38E-ll 1. 13E-05 2.17E-13 1.04E-07 * Grizzly Baghouse was not operating during the 1 st or 2nd quarter of2012, because the Mill's alternate feed circuit was running and no ore was being ground. * * The North Yellowcake Dryer was not in operation during the 4th quarter of2012. 10 N:\WMM\Required Reports\Semi Annual Effluent Reports\2012 July -Dec\July_toDec_2012_SAER_text.docx 6.0 SURFACE WATER MONITORING Under the License, Part 11.2 B surface water samples are required to be obtained annually from Westwater Canyon and semi-annually from Cottonwood Creek. Sediment samples from Westwater Canyon are taken in place of the Westwater Canyon surface water sample in the event that surface water is not available for sampling. Westwater Canyon surface water was not sampled in the third or fourth quarter 2012 because no water was present during this reporting period. However, as required, a sediment sample was collected. The results of the sediment sample are discussed in Section 7 below, and the analytical data is included in Attachment I of this report. The Mill's Environmental Protection Manual requires that Cottonwood Creek be sampled for total dissolved solids ("TDS") and total suspended solids ("TSS") quarterly, and the License, Part 11.2 B requires that Cottonwood Creek be sampled for dissolved and suspended radionuclides including Gross Alpha, Unat, Ra-226, Th-230 semi- annually. In accordance with these requirements, Cottonwood Creek was sampled for TDS, TSS, and all radionuclides during the 3rd quarter. Surface water was not collected from Cottonwood Creek during the 4th quarter of 2012, because there was no surface water present during the quarter. The field data sheets for the surface water sampling events, along with graphs showing historic results are included as Attachment H. The results of this sampling indicate that surface water results remain low and within the range of typical background. 7.0 SOIL SAMPLING Under Tab 4.1 of the Mill's Environmental Protection Manual, surface soils are required to be sampled at the Mill's air monitoring stations (BHV-l, BHV-2, BHV-3, BHV-4, BHV -5 and BHV -6) once per year during August or as soon as possible thereafter, but no later than September 30 of each year. In accordance with the Mill's Environmental Protection Manual, surface soils were collected in August 2012. All soil samples were analyzed, on a dry basis, for Ra-226 and U-nat. Annual soil samples were collected at the six air monitoring stations. The results of these samplings indicate that soils at the air monitoring stations and at Westwater Canyon remain low and within the range of typical background. A graphical presentation of historical results for soils at the air monitoring stations, together with analytical sample results for the August 2012 sampling are provided in Attachment I. 8.0 METEOROLOGICAL MONITORING As in prior reporting periods, an independent contractor has prepared the White Mesa Mill Semi-annual Meteorological Monitoring Report for the period of July through December 2012. This information is retained at the Mill site for agency review. 11 N:\WMM\Required Reports\Semi Annual Effluent Reports\2012 July -Dec\July_toDec_2012_SAER_text.docx 9.0 SIGNATURE This Report was prepared by Energy Fuels Resources (USA) Inc. on February 27,2013. Energy Fuels Resources (USA) Inc. 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MESA, Mll,L --REViSioNS I County: SAN -JUAN --Stale: UT Date By • Location: 11109 dis 1/13/11 I BM 1/27/11 BM High Volume Air Monitoring Stations 3/2112 GM Scale: as shown Author: HRR ATTACHMENT B BHV AIR SAMPLING GRAPHS AND DATA TABLES TAB 1 BHV-l AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-lU Effluent Concentration Limit = 2E-14 uCi/ml BHV-lT Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = 6E-13 uCi/ml BHV-1PB ALARAGoal= 2.2SE-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal= 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 2.3sE-1s s.00E-12 L2sE-12 7.82E-16 8.00E-14 2.00E-14 L06E-1s 2.00E-12 s.OOE-13 2.s7E-14 4.00E-12 LOOE-12 12/14/1981 Ls6E-1s s.00E-12 L2sE-12 L49E-1s 8.00E-14 2.00E-14 L93E-1s 2.00E-12 s.OOE-13 2.64E-14 4.00E-12 LOOE-12 3/29/1982 2.16E-1s s.00E-12 L2sE-12 2.93E-1s 8.00E-14 2.00E-14 1.16E-1s 2.00E-12 s.OOE-13 2.09E-14 4.00E-12 LOOE-12 6/30/1982 4.69E-1s s.00E-12 L2sE-12 3.46E-1s 8.00E-14 2.00E-14 2.38E-1s 2.00E-12 s.OOE-13 2.14E-14 4.00E-12 LOOE-12 9/27/1982 4.4sE-1s s.00E-12 L2sE-12 3.29E-1s 8.00E-14 2.00E-14 3.23E-1s 2.00E-12 s.OOE-13 L99E-14 4.00E-12 LOOE-12 1/3/1983 4.39E-1s s.00E-12 L2sE-12 s.91E-16 8.00E-14 2.00E-14 9.14E-16 2.00E-12 s.OOE-13 4.87E-14 4.00E-12 LOOE-12 4/4/1983 7.51E-16 s.00E-12 L2sE-12 2.13E-16 8.00E-14 2.00E-14 3.20E-16 2.00E-12 s.OOE-13 L88E-14 4.00E-12 LOOE-12 6/30/1983 2.68E-16 s.00E-12 L2sE-12 6.92E-16 8.00E-14 2.00E-14 7.92E-16 2.00E-12 s.OOE-13 2.00E-14 4.00E-12 LOOE-12 10/3/1983 s.00E-12 L2sE-12 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 s.OOE-13 4.00E-12 LOOE-12 1/3/1984 2.87E-1s s.00E-12 L2sE-12 1.14E-16 8.00E-14 2.00E-14 L79E-16 2.00E-12 s.OOE-13 L06E-14 4.00E-12 LOOE-12 4/2/1984 Ls9E-1s s.00E-12 L2sE-12 3.40E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 s.OOE-13 3.34E-14 4.00E-12 LOOE-12 7/2/1984 3.10E-1s s.00E-12 L2sE-12 LOOE-1s 8.00E-14 2.00E-14 2.09E-1s 2.00E-12 s.OOE-13 L88E-14 4.00E-12 LOOE-12 10/1/1984 6.42E-16 s.00E-12 L2sE-12 l.39E-16 8.00E-14 2.00E-14 L94E-16 2.00E-12 s.OOE-13 L8sE-14 4.00E-12 LOOE-12 1/2/1985 s.06E-16 s.00E-12 L2sE-12 4.s6E-16 8.00E-14 2.00E-14 3.49E-16 2.00E-12 s.OOE-13 3.03E-14 4.00E-12 LOOE-12 4/1/1985 O.OOE+OO s.00E-12 L2sE-12 L23E-1s 8.00E-14 2.00E-14 4.88E-16 2.00E-12 s.OOE-13 8.06E-1s 4.00E-12 LOOE-12 7/1/1985 7.17E-16 s.00E-12 L2sE-12 8.00E-14 2.00E-14 LOsE-1s 2.00E-12 s.OOE-13 2.1sE-14 4.00E-12 LOOE-12 9/30/1985 6.13E-16 s.00E-12 L2sE-12 1.18E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 s.OOE-13 3.64E-1s 4.00E-12 LOOE-12 1/2/1986 3.42E-1s s.00E-12 L2sE-12 4.74E-16 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 LOOE-12 4/1/1986 3.98E-1s s.00E-12 L2sE-12 9.74E-16 8.00E-14 2.00E-14 LsOE-1s 2.00E-12 s.OOE-13 L41E-14 4.00E-12 LOOE-12 6/30/1986 s.slE-17 s.00E-12 L2sE-12 3.s2E-16 8.00E-14 2.00E-14 L37E-1s 2.00E-12 s.OOE-13 L23E-14 4.00E-12 LOOE-12 10/27/1986 L99E-1s s.00E-12 L2sE-12 3.06E-16 8.00E-14 2.00E-14 L2sE-1s 2.00E-12 s.OOE-13 L08E-14 4.00E-12 LOOE-12 12/15/1986 L67E-1s s.00E-12 L2sE-12 1.16E-16 8.00E-14 2.00E-14 s.98E-16 2.00E-12 s.OOE-13 L37E-14 4.00E-12 LOOE-12 3/16/1987 2.33E-1s s.00E-12 L2sE-12 4.30E-16 8.00E-14 2.00E-14 L92E-16 2.00E-12 s.OOE-13 s.59E-14 4.00E-12 LOOE-12 5/11/1987 2.36E-1s s.00E-12 L2sE-12 7.69E-16 8.00E-14 2.00E-14 8.76E-16 2.00E-12 s.OOE-13 L4sE-14 4.00E-12 LOOE-12 9/9/1987 2.27E-1s s.00E-12 L2sE-12 2.44E-1s 8.00E-14 2.00E-14 8.s1E-16 2.00E-12 s.OOE-13 3.14E-14 4.00E-12 LOOE-12 11/2/1987 2.7sE-1s s.00E-12 L2sE-12 2.46E-1s 8.00E-14 2.00E-14 l.34E-1s 2.00E-12 s.OOE-13 2.79E-14 4.00E-12 LOOE-12 2/16/1988 L07E-1s s.00E-12 L2sE-12 L47E-16 8.00E-14 2.00E-14 4.44E-16 2.00E-12 s.OOE-13 4.01E-14 4.00E-12 LOOE-12 5/18/1988 L98E-1s s.00E-12 L2sE-12 L2sE-1s 8.00E-14 2.00E-14 6.40E-16 2.00E-12 s.OOE-13 L07E-14 4.00E-12 LOOE-12 8/15/1988 2.06E-1s s.00E-12 L2sE-12 3.41E-1s 8.00E-14 2.00E-14 s.08E-16 2.00E-12 s.OOE-13 L62E-14 4.00E-12 LOOE-12 11/14/1988 3.94E-1s s.00E-12 L2sE-12 2.12E-1s 8.00E-14 2.00E-14 L01E-1s 2.00E-12 s.OOE-13 2.47E-14 4.00E-12 LOOE-12 2/13/1989 L99E-1s s.00E-12 L2sE-12 s.73E-16 8.00E-14 2.00E-14 s.99E-16 2.00E-12 s.OOE-13 3.23E-14 4.00E-12 LOOE-12 5/15/1989 L70E-1s s.00E-12 L2sE-12 6.32E-16 8.00E-14 2.00E-14 s.86E-16 2.00E-12 s.OOE-13 6.16E-1s 4.00E-12 LOOE-12 8/14/1989 2.31E-1s s.00E-12 1.2sE-12 2.31E-16 8.00E-14 2.00E-14 L77E-16 2.00E-12 s.OOE-13 7.6sE-1s 4.00E-12 LOOE-12 11/13/1989 4.72E-1s s.00E-12 L2sE-12 L71E-1s 8.00E-14 2.00E-14 Ls2E-1s 2.00E-12 s.OOE-13 L89E-14 4.00E-12 LOOE-12 2/12/1990 3.44E-16 s.00E-12 L2sE-12 8.39E-16 8.00E-14 2.00E-14 8.31E-16 2.00E-12 s.OOE-13 2.57E-14 4.00E-12 LOOE-12 5/14/1990 3.03E-1s s.00E-12 L2sE-12 L47E-1s 8.00E-14 2.00E-14 L04E-1s 2.00E-12 s.OOE-13 L79E-14 4.00E-12 LOOE-12 8/13/1990 L64E-1s s.00E-12 L2sE-12 L49E-1s 8.00E-14 2.00E-14 3.34E-16 2.00E-12 s.OOE-13 8.27E-1s 4.00E-12 LOOE-12 11/12/1990 L48E-1s s.00E-12 L2sE-12 7.s0E-16 8.00E-14 2.00E-14 s.80E-16 2.00E-12 s.OOE-13 2.16E-14 4.00E-12 LOOE-12 2/11/1991 L90E-16 s.00E-12 L2sE-12 3.48E-17 8.00E-14 2.00E-14 7.91E-17 2.00E-12 s.OOE-13 3.79E-14 4.00E-12 LOOE-12 5/13/1991 3.42E-16 s.00E-12 L2sE-12 l.34E-1s 8.00E-14 2.00E-14 7.39E-16 2.00E-12 s.OOE-13 L46E-14 4.00E-12 LOOE-12 8/12/1991 2.77E-16 s.00E-12 L2sE-12 4.17E-17 8.00E-14 2.00E-14 L4sE-16 2.00E-12 s.OOE-13 L80E-14 4.00E-12 LOOE-12 11/11/1991 6.6sE-17 s.00E-12 L2sE-12 9.13E-17 8.00E-14 2.00E-14 2.77E-17 2.00E-12 s.OOE-13 L06E-14 4.00E-12 LOOE-12 2/10/1992 L94E-16 s.00E-12 L2sE-12 4.28E-17 8.00E-14 2.00E-14 4.08E-17 2.00E-12 s.OOE-13 3.s1E-14 4.00E-12 LOOE-12 5/11/1992 2.s4E-16 s.00E-12 L2sE-12 6.49E-16 8.00E-14 2.00E-14 6.86E-17 2.00E-12 s.OOE-13 l.38E-14 4.00E-12 LOOE-12 8/10/1992 L73E-16 s.00E-12 L2sE-12 LssE-16 8.00E-14 2.00E-14 L20E-16 2.00E-12 s.OOE-13 Ls3E-14 4.00E-12 LOOE-12 11/9/1992 Ls6E-16 s.00E-12 L2sE-12 3.19E-17 8.00E-14 2.00E-14 4.90E-18 2.00E-12 s.OOE-13 L86E-14 4.00E-12 LOOE-12 2/9/1993 2.10E-16 s.00E-12 L2sE-12 8.00E-14 2.00E-14 3.89E-17 2.00E-12 s.OOE-13 2.s2E-14 4.00E-12 LOOE-12 5/10/1993 LOOE-16 s.00E-12 L2sE-12 4.11E-17 8.00E-14 2.00E-14 6.43E-17 2.00E-12 s.OOE-13 L26E-14 4.00E-12 LOOE-12 8/10/1993 2.30E-16 s.00E-12 L2sE-12 6.00E-17 8.00E-14 2.00E-14 6.43E-17 2.00E-12 s.OOE-13 L60E-14 4.00E-12 LOOE-12 . 11/8/1993 s.00E-12 L2sE-12 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 s.OOE-13 Ls7E-14 4.00E-12 LOOE-12 i 2/7/1994 L82E-16 s.00E-12 L2sE-12 s.00E-18 8.00E-14 2.00E-14 4.30E-17 2.00E-12 s.OOE-13 2.59E-14 4.00E-12 LOOE-12 5/9/1994 3.60E-16 s.00E-12 L2sE-12 2.70E-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 s.OOE-13 L60E-14 4.00E-12 LOOE-12 8/9/1994 4.04E-16 s.00E-12 L2sE-12 2.70E-16 8.00E-14 2.00E-14 2.94E-16 2.00E-12 s.OOE-13 2.00E-1s 4.00E-12 LOOE-12 11/7/1994 9.18E-17 s.00E-12 L2sE-12 3.60E-16 8.00E-14 2.00E-14 2.91E-16 2.00E-12 s.OOE-13 2.00E-1s 4.00E-12 LOOE-12 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-1U Effluent Concentration Limit = 2E-14 uCi/ml BHV-1T Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = 6E-13 uCi/ml BHV-1PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 l.77E-16 9.00E-14 2.2sE-14 9.70E-17 2.00E-14 s.00E-1s 9.70E-17 9.00E-13 2.2sE-13 8.60E-1s 6.00E-13 l.sOE-13 5/9/1995 9.40E-17 9.00E-14 2.2sE-14 s.36E-16 2.00E-14 s.00E-1s l.60E-1s 9.00E-13 2.2sE-13 3.84E-1s 6.00E-13 l.sOE-13 8/9/1995 2.70E-16 9.00E-14 2.2sE-14 l.60E-16 2.00E-14 s.00E-1s 2.76E-16 9.00E-13 2.2sE-13 3.76E-1s 6.00E-13 l.sOE-13 11/11/1995 4.80E-1s 9.00E-14 2.2sE-14 6.41E-16 2.00E-14 s.00E-1s 8.93E-16 9.00E-13 2.2sE-13 s.20E-1s 6.00E-13 l.sOE-13 2/5/1996 s.34E-1s 9.00E-14 2.2sE-14 2.30E-1s 2.00E-14 s.00E-1s l.30E-1s 9.00E-13 2.2sE-13 4.20E-1s 6.00E-13 l.sOE-13 5/6/1996 s.l1E-16 9.00E-14 2.2sE-14 3.06E-16 2.00E-14 s.00E-1s l.40E-16 9.00E-13 2.2sE-13 7.03E-1s 6.00E-13 1.s0E-13 8/5/1996 s.99E-16 9.00E-14 2.2sE-14 l.ssE-1s 2.00E-14 s.00E-1s 2.03E-16 9.00E-13 2.2sE-13 s.94E-1s 6.00E-13 l.sOE-13 11/6/1996 3.38E-16 9.00E-14 2.2sE-14 s.4sE-16 2.00E-14 s.00E-1s l.00E-16 9.00E-13 2.2sE-13 l.22E-14 6.00E-13 l.sOE-13 2/6/1.997 l.00E-16 9.00E-14 2.2sE-14 l.2sE-16 2.00E-14 s.00E-1s l.28E-16 9.00E-13 2.2sE-13 s.68E-1s 6.00E-13 l.sOE-13 5/5/1997 l.09E-16 9.00E-14 2.2sE-14 l.00E-16 2.00E-14 s.00E-1s l.00E-16 9.00E-13 2.2sE-13 4.39E-1s 6.00E-13 l.sOE-13 8/11/1997 2.88E-16 9.00E-14 2.2sE-14 3.83E-16 2.00E-14 s.00E-1S l.82E-16 9.00E-13 2.2sE-13 S.29E-1s 6.00E-13 l.sOE-13 1/5/1998 3.24E-16 9.00E-14 2.2sE-14 3.47E-16 2.00E-14 S.00E-1s 1.19E-16 9.00E-13 2.2SE-13 4.73E-1S 6.00E-13 l.SOE-13 4/28/1998 4.7SE-16 9.00E-14 2.2SE-14 6.73E-16 2.00E-14 S.00E-1S S.69E-16 9.00E-13 2.2SE-13 S.94E-1S 6.00E-13 l.SOE-13 7/31/1998 8.84E-16 9.00E-14 2.2SE-14 l.93E-1S 2.00E-14 S.00E-1S l.43E-1S 9.00E-13 2.2SE-13 S.22E-1s 6.00E-13 l.sOE-13 9/28/1998 2.81E-16 9.00E-14 2.2SE-14 2.89E-16 2.00E-14 S.00E-1S l.80E-16 9.00E-13 2.2SE-13 4.64E-1S 6.00E-13 l.SOE-13 12/28/1998 8.08E-16 9.00E-14 2.2SE-14 4.93E-16 2.00E-14 S.00E-1S S.01E-16 9.00E-13 2.2SE-13 l.06E-14 6.00E-13 l.SOE-13 3/29/1999 2.06E-16 9.00E-14 2.2SE-14 2.06E-16 2.00E-14 S.00E-1S l.42E-16 9.00E-13 2.2SE-13 6.69E-1s 6.00E-13 l.SOE-13 7/3/1999 S.31E-16 9.00E-14 2.2SE-14 2.47E-16 2.00E-14 s.00E-1S 2.23E-16 9.00E-13 2.2SE-13 6.44E-1S 6.00E-13 l.SOE-13 9/27/1999 8.98E-16 9.00E-14 2.2SE-14 3.90E-16 2.00E-14 S.00E-1S 2.96E-16 9.00E-13 2.2SE-13 7.29E-1S 6.00E-13 l.SOE-13 12/28/1999 l.48E-1s 9.00E-14 2.2SE-14 6.00E-16 2.00E-14 S.00E-1S S.57E-16 9.00E-13 2.2SE-13 6.19E-1S 6.00E-13 l.sOE-13 3/27/2000 1.00E-16 9.00E-14 2.2SE-14 1.06E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.23E-1S 6.00E-13 l.SOE-13 6/26/2000 3.47E-16 9.00E-14 2.2SE-14 3.46E-16 2.00E-14 S.00E-1S 3.62E-16 9.00E-13 2.2SE-13 4.S0E-1S 6.00E-13 l.sOE-13 9/26/2000 2.S1E-16 9.00E-14 2.2SE-14 l.78E-16 2.00E-14 S.00E-1S 3.2SE-16 9.00E-13 2.2SE-13 8.sSE-1S 6.00E-13 l.SOE-13 12/26/2000 l.00E-16 9.00E-14 2.2SE-14 l.42E-16 2.00E-14 S.00E-1S l.31E-16 9.00E-13 2.2sE-13 7.77E-1s 6.00E-13 l.SOE-13 3/26/2001 3.lOE-16 9.00E-14 2.2SE-14 l.00E-1s 2.00E-14 S.00E-1S l.00E-1S 9.00E-13 2.2SE-13 7.19E-1S 6.00E-13 l.SOE-13 7/29/2001 l.S2E-16 9.00E-14 2.2SE-14 l.44E-16 2.00E-14 S.00E-1s l.77E-16 9.00E-13 2.2SE-13 7.21E-1s 6.00E-13 l.sOE-13 9/24/2001 l.03E-16 9.00E-14 2.2SE-14 l.00E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2sE-13 8.09E-1S 6.00E-13 l.sOE-13 12/31/2001 1.00E-16 9.00E-14 2.2sE-14 l.00E-16 2.00E-14 S.00E-1s l.00E-16 9.00E-13 2.2SE-13 l.39E-1S 6.00E-13 l.sOE-13 4/1/2002 2.0SE-16 9.00E-14 2.2SE-14 2.44E-16 2.00E-14 S.00E-1S 2.29E-16 9.00E-13 2.2SE-13 8.1SE-1S 6.00E-13 l.SOE-13 7/1/2002 3.SsE-16 9.00E-14 2.2SE-14 4.8SE-16 2.00E-14 s.00E-1S l.06E-16 9.00E-13 2.2SE-13 7.6SE-1S 6.00E-13 l.SOE-13 9/30/2002 1.17E-16 9.00E-14 2.2SE-14 l.61E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 3.68E-1S 6.00E-13 l.S0E-13 12/30/2002 l.00E-16 9.00E-14 2.2SE-14 l.03E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 9.46E-1S 6.00E-13 l.s0E-13 3/31/2003 1.20E-16 9.00E-14 2.2SE-14 1.12E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 4.68E-1S 6.00E-13 l.SOE-13 6/30/2003 2.18E-16 9.00E-14 2.2SE-14 3.40E-16 2.00E-14 S.00E-1S 1.67E-16 9.00E-13 2.2SE-13 s.96E-1s 6.00E-13 l.S0E-13 9/29/2003 l.00E-16 9.00E-14 2.2SE-14 l.00E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 7.28E-1S 6.00E-13 l.S0E-13 12/29/2003 l.00E-16 9.00E-14 2.2SE-14 2.54E-16 2.00E-14 S.00E-1s 3.3SE-16 9.00E-13 2.2SE-13 6.2SE-1S 6.00E-13 l.S0E-13 3/29/2004 l.00E-16 9.00E-14 2.2SE-14 l.00E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 l.S4E-14 6.00E-13 l.S0E-13 6/27/2004 l.00E-16 9.00E-14 2.2SE-14 l.00E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 3.04E-1S 6.00E-13 l.S0E-13 9/27/2004 l.00E-16 9.00E-14 2.2SE-14 l.00E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 l.OsE-14 6.00E-13 l.s0E-13 12/27/2004 l.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 S.00E-1s l.00E-16 9.00E-13 2.2sE-13 l.S9E-14 6.00E-13 l.s0E-13 3/28/200S l.00E-16 9.00E-14 2.2SE-14 l.00E-16 2.00E-14 s.00E-1S l.00E-16 9.00E-13 2.2sE-13 7.42E-1S 6.00E-13 l.s0E-13 6/29/2005 l.00E-16 9.00E-14 2.2SE-14 l.30E-16 2.00E-14 s.00E-1S l.20E-16 9.00E-13 2.2sE-13 7.94E-1s 6.00E-13 l.S0E-13 9/26/2005 l.00E-16 9.00E-14 2.2SE-14 2.S6E-16 2.00E-14 s.00E-1S 2.42E-16 9.00E-13 2.2sE-13 l.22E-14 6.00E-13 l.S0E-13 1/3/2006 2.13E-16 9.00E-14 2.2SE-14 l.04E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 3.73E-14 6.00E-13 l.SOE-13 4/3/2006 1.62E-16 9.00E-14 2.2SE-14 l.86E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 8.36E-1S 6.00E-13 l.SOE-13 7/3/2006 l.86E-16 9.00E-14 2.2SE-14 l.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 9.77E-1S 6.00E-13 l.S0E-13 10/2/2006 l.00E-16 9.00E-14 2.2SE-14 l.00E-16 2.00E-14 S.00E-1s l.00E-16 9.00E-13 2.2SE-13 l.30E-14 6.00E-13 l.S0E-13 1/1/2007 l.00E-16 9.00E-14 2.2sE-14 l.47E-16 2.00E-14 s.00E-1s l.00E-16 9.00E-13 2.2sE-13 1.17E-14 6.00E-13 l.s0E-13 4/2/2007 2.23E-16 9.00E-14 2.2sE-14 l.63E-16 2.00E-14 s.00E-1S l.00E-16 9.00E-13 2.2SE-13 1.6SE-14 6.00E-13 l.S0E-13 7/2/2007 3.3sE-16 9.00E-14 2.2sE-14 l.34E-16 2.00E-14 s.00E-1s l.36E-16 9.00E-13 2.2sE-13 1.78E-14 6.00E-13 l.S0E-13 9/30/2007 l.lSE-16 9.00E-14 2.2SE-14 l.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 7.68E-1S 6.00E-13 l.s0E-13 12/31/2007 l.00E-16 9.00E-14 2.2SE-14 l.93E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2sE-13 l.31E-14 6.00E-13 l.SOE-13 3/31/2008 1.14E-16 9.00E-14 2.2SE-14 l.13E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 6.44E-1S 6.00E-13 l.S0E-13 6/30/2008 7.09E-16 9.00E-14 2.2sE-14 3.83E-16 2.00E-14 S.00E-1S 2.27E-16 9.00E-13 2.2SE-13 6.s2E-1S 6.00E-13 l.sOE-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-lU Effluent Concentration Limit = 2E-14 uCi/ml BHV-lT Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = 6E-13 uCi/ml BHV-1PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal= 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 7.69E-16 9.00E-14 2.2SE-14 2.94E-16 2.00E-14 S.00E-1S L90E-16 9.00E-13 2.2SE-13 7.64E-1S 6.00E-13 LSOE-13 12/31/2008 L21E-1S 9.00E-14 2.2SE-14 4.76E-16 2.00E-14 S.00E-1S 3.34E-16 9.00E-13 2.2SE-13 1.16E-14 6.00E-13 LSOE-13 3/15/2009 2.14E-1S 9.00E-14 2.2SE-14 L02E-1S 2.00E-14 S.00E-1S LOOE-1S 9.00E-13 2.2SE-13 4.44E-1S 6.00E-13 LSOE-13 6/15/2009 S.97E-17 9.00E-14 2.2SE-14 2.3SE-16 2.00E-14 S.00E-1S 2.18E-16 9.00E-13 2.2SE-13 S.13E-1S 6.00E-13 LSOE-13 9/15/2009 9.SSE-16 9.00E-14 2.2SE-14 L71E-16 2.00E-14 S.00E-1S 9.87E-17 9.00E-13 2.2SE-13 9.47E-1S 6.00E-13 1.S0E-13 12/15/2009 1.24E-1S 9.00E-14 2.2SE-14 9.2SE-17 2.00E-14 S.00E-1S S.60E-17 9.00E-13 2.2SE-13 S.9SE-1S 6.00E-13 1.S0E-13 3/31/2010 1.97E-1S 9.00E-14 2.2SE-14 2.1SE-16 2.00E-14 S.00E-1S 3.27E-16 9.00E-13 2.2SE-13 1.00E-14 6.00E-13 l.S0E-13 6/30/2010 1.S8E-1S 9.00E-14 2.2SE-14 4.71E-16 2.00E-14 S.00E-1S 7.70E-16 9.00E-13 2.2SE-13 4.07E-1S 6.00E-13 1.S0E-13 9/30/2010 8.42E-16 9.00E-14 2.2SE-14 2.80E-16 2.00E-14 S.00E-1S l.31E-16 9.00E-13 2.2SE-13 6.80E-1S 6.00E-13 1.S0E-13 12/31/2010 l.27E-1S 9.00E-14 2.2SE-14 2.32E-16 2.00E-14 S.00E-1S 2.30E-16 9.00E-13 2.2SE-13 l.27E-14 6.00E-13 1.S0E-13 4/4/2011 9.01E-16 9.00E-14 2.2SE-14 1.90E-16 2.00E-14 S.00E-1S 3.64E-16 9.00E-13 2.2SE-13 1.09E-14 6.00E-13 1.S0E-13 7/4/2011 l.S9E-1S 9.00E-14 2.2SE-14 S.31E-16 2.00E-14 S.00E-1S 4.99E-16 9.00E-13 2.2SE-13 8.38E-1S 6.00E-13 1.S0E-13 10/3/2011 2.92E-16 9.00E-14 2.2SE-14 1.17E-16 2.00E-14 S.00E-1S 6.76E-17 9.00E-13 2.2SE-13 1.14E-14 6.00E-13 1.S0E-13 1/3/2012 6.73E-16 9.00E-14 2.2SE-14 1.19E-16 2.00E-14 S.00E-1S 8.S8E-17 9.00E-13 2.2SE-13 L73E-14 6.00E-13 1.S0E-13 4/3/2012 7.87E-16 9.00E-14 2.2SE-14 2.64E-16 2.00E-14 S.00E-1S 3.9SE-16 9.00E-13 2.2SE-13 l.2SE-14 6.00E-13 1.S0E-13 7/2/2012 1.86E-1S 9.00E-14 2.2SE-14 8.33E-16 2.00E-14 S.00E-1S 9.8SE-16 9.00E-13 2.2SE-13 9.SSE-1S 6.00E-13 1.S0E-13 10/1/2012 1.06E-1S 9.00E-14 2.2SE-14 2.11E-16 2.00E-14 S.00E-1S 2.34E-16 9.00E-13 2.2SE-13 1. 13 E-14 6.00E-13 1.S0E-13 12/31/2012 6.86E-16 9.00E-14 2.2SE-14 1.27E-16 2.00E-14 S.00E-1S 1.38E-16 9.00E-13 2.2SE-13 1.S4E-14 6.00E-13 1.S0E-13 -E :::: o :::l -til t: o ~ co '-.... t: (l) (J t: o ,0 (l) "C (J :::l t: .2 "C co c::: ~ I > ::I: m N T""" I W 0 ~ ('I') T""" I W 0 ~ T""" -. l~ I- ~ • ~ I~ -~ --r-.. ~ +c:: ~ • .... .::: t!. ~ ~ I· ::::::: ~ ~ :::; ~ «:; ~ ...... ~ ~~ l ~ t:::::.. .. -~ .. ~ ~ ~ ~ :::::::: I· 1'-4 ~~ F: ~. l ~ T""" I W 0 ~ ac:::1 ....4l1lI ,.....-. Z~-des .r-. -:::.~ ~ .-:::::::::: I"~ i: ~ ~ ~r--.:: ~ i--~~ ~ ~~ I.,. r-~_ --.: ~~ ~ ~ ~-:;;;~ ~ i" ~ ~ ~ ~ ~ ~-des o~-des 60-des go-des LO-deS go-des 90-des -~ ~ ~ ~ I· ..-; ~ ~~ ~ ~ ... r-: r::.~ ~ ~-I-~ "'WI ~ ::::.a ~ - vo-des 0 T""" N £O-deS I "'0 ro Q) zo-des ....J + ~o-des ~ .111:: ~;~ ~ !!: • ~ .... ........ .~ ~ ~ ~ r-~ I ~~: '"" ~ ~ .~ ... '-/ ~ ::.1 ~~ 6c:::: ~~ '"" l i.'!! -~, '"" -:::::;:. ~ ~~ -I!"""'" --= ~~ If: -. r" • ~ ~ ~ ,~ L i:-4 "'" oo-des CD N N I 66-deS E .:2 96-deS "'0 ro c::: L6-deS + 96-deS 0 ('I) 96-deS N I E v6-deS :::l ·c 0 £6-deS ..c ..... Z6-deS + '""-r'I:::::~ .... ~6-des ro ~ :::l .... '"" ~ ~ ~~ 06-deS ro z I""~ ~ .... ~ ~ ~''''" ~~ ~ a-...... .~~ :::::=. It --!: :. .... ~~I"'"" ~ ~ ~ 69-deS E :::l gg-deS c ro ~ ::) L9-deS + gg-deS ~"-"Y r-~;-r--r-+ ~ ~ ~-• """'!!II ........ "" 99-deS vg-deS -~-..-~ ... £g-deS i i ~ Zg-deS F:lII ~ ~g-des LO CD l"-co T""" T""" T""" T""" I I I I W W W W 0 0 0 0 ~ ~ ~ ~ T""" (ele~s 601) 1.00E-11 1.00E-12 1.00E-13 (i) ro ~ .OOE-1 4 Q) o --.J '-'" 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml Y94 ... , I' .. 'ff ]{ /1 BHV-1 Uranium-Natural Concentrations (uCi/ml) .• .J. ," I fH.~\". 1\ .. ¥ , J¥ 'l ~ .. ~ I "1\~ 'h. -..... .... I " -. ~ At"[ -1 I A I T .... \ J1' 1 1 .1 \ ~..,. ~ V \ / • Ai. 11 • V ~ Jt.. •• J ,~ J _ T • .ll I; 1\ 1. • l\ .. .. \T~· W V ~ V V lJ\ J~ u T""" N (V) .q LO CD I"-ex:> (J) 0 T""" N (V) .q LO CD I"-ex:> (J) 0 T""" N (V) .q LO CD I"-ex:> (J) 0 N ex:> ex:> ex:> ex:> ex:> ex:> ex:> ex:> ex:> (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) 0 0 0 0 0 0 0 0 0 0 T""" T""" T""" I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) -E :-:::: () ::l -tn c: o +::i l! .... c: (1) (.) c: o () o M N I E ::l "L: o ~ I- ~ I > ::I: m N ~ I W o o ('t") ~ I W 0 ~ " -~ ~ ~ I W 0 ~ --f-H -r-~ ~-= I-r- tc ~~ ... ~ .. ~ ~ - I~ I· I· f:::: !PI-r+ +-~ I.F:: '-:1'-., ~~ I '~ t;: ---i"-r--t_ -+== "r- .0::::;;;;;;;:.. I- ~Oc ~:::: ~t: I--- .... ~ 15 ~~ fo--~ i.~ ~ r-..... ..... w: r--1-1-4 I-r- ... ~~ r-.., r-t--.. t-t-\tro-t-- t-t-t-.. r- • ~ .. +-f-~ I~I--~ ~ r+- L() ~ I W 0 0 (ele~s 001) ,...--.. t::t ~ [;:::= ~ ~ ~ ~ [;j D ~ I:::::::-iI A .. ==- ....- ~ ~ ~ ~ ~ CD ~ I W 0 ~ I~~ ~. :..1..4 I--~ I--l::~ t- ~ I W 0 ~ ~ ~ oo ~ I W 0 ~ l~-des ~ ~-des o~-des 60-deS so-des Lo-des go-des go-des vO-deS £O-deS lO-deS ~o-des oo-des 66-deS S6-des L6-des 96-deS 96-deS v6-deS £6-deS l6-des ~6-des 06-deS 6s-des ss-des LS-deS gs-des 9S-deS vs-des £s-des ls-des ~s-des 1.00E-11 1.00E-12 1.00E-13 ~.OOE-1 4 Q) ro u CJ) 0) o --l -r.OOE-15 1.00E-16 1.00E-17 1.00E-18 Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/m I • .\ • 1fJ\ A .. ~ t ~ ... ... .J. "" \r'llllL ......... \ ... II ." \ • '0" \ \I ~ ., • IF \ \ • \ I V V ~ \ • J .... • u 1 I .ill.. 'T • ~ N ("f) .q-LO <0 I"-00 0) 0 ~ 00 00 00 00 00 00 00 00 00 0) 0) I I I I I I I I I I I Q. Q. Q. Q. Q. Q. Q. Q. Q. Q. Q. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) \ .. \ , ........ n i~ \ I ~ . T I N ("f) .q- 0) 0) 0) I I I Q. Q. Q. Q) Q) Q) CJ) CJ) CJ) BHV-1 Radium-226 Concentrations (uCi/ml) r It 1 ... .... I ... ~ \ T /I \ \ .1'1 .J.. \ V I 1\ .l' .. \ • 6' 6 " T , • ... I V \ .. / \ \ . /\ ~ .J. I • I • JI\tJ'J ~ ~ ~ ¥ \jUJLJLJJ'" \ ~ I ~ .. LO <0 I"-00 0) 0 ~ N ("f) .q-LO <0 I"-00 0) 0 N 0) 0) 0) 0) 0) 0 0 0 0 0 0 0 0 0 0 ~ ~ ~ I I I I I I I I I I I I I I I I I I Q. Q. Q. Q. Q. Q. Q. Q. Q. Q. Q. Q. Q. Q. Q. Q. Q. Q. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) 1.00E-11 1.00E-12 1.00E-13 Q) co u Cf.1.00E-14 0) o ....J ........... 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1 E-12 uCi/ml .... "JI" II ...... BHV-1 Lead-210 Concentrations (uCi/ml) , I 1\ ....... .J{. X'. 1 ~ L /\" 4 I r \ 11 .A ~ \ 1\ Jt ~ I' " T~l"\~";~ \f T'/~V~~ t .l~JlJil1~ •...... ~AJ u ~" ...... I --... I , \ .M"'a. _ \ IllY' \ ./'F-.r .. JPaI 'I , vr \£T\I \.~ • ~ ~ • u.. fir Jl • .... I • 1 .... 11 II .... , ~ N C"0 ~ L() <0 t-co 0) 0 ~ N C"0 ~ L() <0 t-co 0) 0 ~ N C"0 ~ L() <0 t-co 0) 0 N co co co co co co co co co 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0 0 0 0 0 0 0 0 0 0 ~ ~ ~ I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) TAB 2 BHV-2 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration limit = 9E-14 uCi/ml BHV-2U Effluent Concentration limit = 2E-14 uCi/ml BHV-2T Effluent Concentration limit = 9E-13 uCi/ml BHV-2R Effluent Concentration limit = 6E-13 uCi/ml BHV-2PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC limit = SE-12 uCi/ml Pre 1994 MPC limit = 8E-14 uCi/ml Pre 1994 MPC limit = 2E-12 uCi/ml Pre 1994 MPC limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 1.39E-ls s.00E-12 L2SE-12 3.69E-16 8.00E-14 2.00E-14 s.92E-16 2.00E-12 s.OOE-13 L67E-14 4.00E-12 LOOE-12 12/14/1981 4.62E-16 s.00E-12 1.2sE-12 8.03E-16 8.00E-14 2.00E-14 3.62E-16 2.00E-12 s.OOE-13 L33E-14 4.00E-12 LOOE-12 3/29/1982 7.07E-16 s.00E-12 L2sE-12 l.10E-ls 8.00E-14 2.00E-14 7.27E-16 2.00E-12 s.OOE-13 Ls2E-14 4.00E-12 LOOE-12 6/30/1982 8.84E-16 S.00E-12 L2sE-12 7.73E-16 8.00E-14 2.00E-14 4.78E-16 2.00E-12 S.OOE-13 L98E-14 4.00E-12 LOOE-12 9/27/1982 L23E-ls S.00E-12 L2sE-12 3.60E-16 8.00E-14 2.00E-14 8.73E-16 2.00E-12 S.OOE-13 2.3SE-14 4.00E-12 LOOE-12 1/3/1983 2.64E-ls s.00E-12 1.2sE-12 2.5sE-16 8.00E-14 2.00E-14 L98E-16 2.00E-12 s.OOE-13 2.8sE-14 4.00E-12 LOOE-12 4/4/1983 2.14E-16 s.00E-12 L2sE-12 L02E-16 8.00E-14 2.00E-14 Ls7E-16 2.00E-12 s.OOE-13 2.48E-14 4.00E-12 LOOE-12 6/30/1983 2.8sE-16 s.00E-12 1.2sE-12 2.06E-16 8.00E-14 2.00E-14 2.24E-16 2.00E-12 s.OOE-13 L79E-14 4.00E-12 LOOE-12 10/3/1983 2.70E-16 s.00E-12 L2sE-12 3.36E-16 8.00E-14 2.00E-14 4.37E-16 2.00E-12 S.OOE-13 L78E-14 4.00E-12 LOOE-12 1/3/1984 2.78E-ls s.00E-12 L2sE-12 1.20E-16 8.00E-14 2.00E-14 6.64E-17 2.00E-12 S.OOE-13 9.14E-ls 4.00E-12 LOOE-12 4/2/1984 4.28E-16 s.00E-12 L2SE-12 L7sE-16 8.00E-14 2.00E-14 4.57E-17 2.00E-12 s.OOE-13 3.SsE-14 4.00E-12 LOOE-12 7/2/1984 2.78E-ls s.00E-12 1.2sE-12 8.12E-16 8.00E-14 2.00E-14 L98E-16 2.00E-12 s.OOE-13 L68E-14 4.00E-12 LOOE-12 10/1/1984 2.69E-16 S.00E-12 L2SE-12 2.66E-17 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 s.OOE-13 L77E-14 4.00E-12 LOOE-12 1/2/1985 2.1sE-16 S.00E-12 L2SE-12 7.SSE-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 s.OOE-13 3.19E-14 4.00E-12 LOOE-12 4/1/1985 LOOE-16 S.00E-12 L2sE-12 L67E-16 8.00E-14 2.00E-14 6.7sE-17 2.00E-12 s.OOE-13 7.S6E-ls 4.00E-12 LOOE-12 7/1/1985 3.70E-17 s.00E-12 1.2SE-12 9.00E-16 8.00E-14 2.00E-14 4.90E-17 2.00E-12 S.OOE-13 1.31E-14 4.00E-12 LOOE-12 9/30/1985 9.32E-17 s.00E-12 L2sE-12 2.18E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 s.00E-13 3.64E-ls 4.00E-12 LOOE-12 1/2/1986 LOOE-16 s.OOE-12 L2sE-12 2.16E-16 8.00E-14 2.00E-14 2.1sE-17 2.00E-12 s.OOE-13 3.04E-16 4.00E-12 LOOE-12 4/1/1986 1.31E-ls S.00E-12 L2SE-12 LsOE-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 s.OOE-13 2.90E-ls 4.00E-12 LOOE-12 6/30/1986 2.23E-16 S.00E-12 1.2sE-12 1.32E-16 8.00E-14 2.00E-14 7.09E-17 2.00E-12 S.OOE-13 2.53E-14 4.00E-12 LOOE-12 10/27/1986 6.41E-16 s.00E-12 L2sE-12 L74E-16 8.00E-14 2.00E-14 3.67E-16 2.00E-12 s.00E-13 L04E-14 4.00E-12 LOOE-12 12/15/1986 3.s6E-16 s.00E-12 L2sE-12 LOOE-16 8.00E-14 2.00E-14 LOsE-16 2.00E-12 s.OOE-13 7.81E-ls 4.00E-12 LOOE-12 3/16/1987 s.31E-16 s.00E-12 L2sE-12 1.30E-16 8.00E-14 2.00E-14 7.74E-17 2.00E-12 s.OOE-13 3.80E-14 4.00E-12 LOOE-12 5/11/1987 4.06E-16 S.00E-12 L2SE-12 6.63E-17 8.00E-14 2.00E-14 1.34E-16 2.00E-12 S.OOE-13 l.10E-14 4.00E-12 LOOE-12 9/9/1987 2.74E-16 S.00E-12 1.2sE-12 2.38E-16 8.00E-14 2.00E-14 1.38E-16 2.00E-12 s.OOE-13 L04E-14 4.00E-12 LOOE-12 11/2/1987 3.73E-16 s.00E-12 1.2SE-12 3.11E-16 8.00E-14 2.00E-14 L83E-16 2.00E-12 s.OOE-13 l.17E-14 4.00E-12 LOOE-12 2/16/1988 2.78E-ls S.00E-12 L2SE-12 2.31E-17 8.00E-14 2.00E-14 L20E-16 2.00E-12 s.OOE-13 3.SSE-14 4.00E-12 LOOE-12 5/18/1988 4.63E-16 s.00E-12 1.2SE-12 L49E-16 8.00E-14 2.00E-14 2.30E-16 2.00E-12 s.OOE-13 L18E-14 4.00E-12 LOOE-12 8/15/1988 8.06E-16 s.00E-12 1.2SE-12 8.69E-16 8.00E-14 2.00E-14 L80E-16 2.00E-12 s.OOE-13 L42E-14 4.00E-12 LOOE-12 11/14/1988 4.34E-16 s.00E-12 L2sE-12 6.76E-16 8.00E-14 2.00E-14 Ls7E-16 2.00E-12 s.OOE-13 2.2sE-14 4.00E-12 LOOE-12 2/13/1989 s.80E-16 s.00E-12 L2sE-12 2.8sE-16 8.00E-14 2.00E-14 LssE-16 2.00E-12 s.OOE-13 2.80E-14 4.00E-12 LOOE-12 5/15/1989 s.06E-16 s.00E-12 1.2sE-12 2.28E-16 8.00E-14 2.00E-14 L63E-16 2.00E-12 S.OOE-13 6.0sE-1S 4.00E-12 LOOE-12 8/14/1989 4.71E-16 S.00E-12 L2sE-12 9.60E-16 8.00E-14 2.00E-14 L26E-1S 2.00E-12 S.OOE-13 6.6SE-1S 4.00E-12 LOOE-12 11/13/1989 l.14E-ls s.00E-12 L2sE-12 4.08E-16 8.00E-14 2.00E-14 4.18E-16 2.00E-12 S.OOE-13 Ls9E-14 4.00E-12 LOOE-12 2/12/1990 L09E-ls S.00E-12 L2sE-12 3.2SE-16 8.00E-14 2.00E-14 3.74E-16 2.00E-12 s.OOE-13 L98E-14 4.00E-12 LOOE-12 5/14/1990 9.32E-16 S.00E-12 L2sE-12 S.27E-16 8.00E-14 2.00E-14 3.97E-16 2.00E-12 S.OOE-13 L69E-14 4.00E-12 LOOE-12 I 8/13/1990 L66E-16 S.00E-12 L2SE-12 S.49E-16 8.00E-14 2.00E-14 4.75E-17 2.00E-12 S.OOE-13 L27E-1S 4.00E-12 LOOE-12 11/12/1990 6.0sE-16 s.00E-12 L2sE-12 2.64E-16 8.00E-14 2.00E-14 L93E-16 2.00E-12 S.OOE-13 2.2SE-14 4.00E-12 LOOE-12 I 2/11/1991 8.72E-17 S.00E-12 1.2sE-12 7.00E-18 8.00E-14 2.00E-14 3.33E-17 2.00E-12 s.OOE-13 3.49E-14 4.00E-12 LOOE-12 5/13/1991 l.16E-16 s.00E-12 L2sE-12 3.86E-16 8.00E-14 2.00E-14 2.80E-16 2.00E-12 s.OOE-13 LsOE-14 4.00E-12 LOOE-12 8/12/1991 9.02E-17 S.00E-12 L2SE-12 8.82E-17 8.00E-14 2.00E-14 7.6sE-17 2.00E-12 s.OOE-13 LS8E-14 4.00E-12 LOOE-12 11/11/1991 4.81E-17 S.00E-12 L2sE-12 3.82E-17 8.00E-14 2.00E-14 2.54E-17 2.00E-12 s.OOE-13 L4sE-14 4.00E-12 LOOE-12 2/10/1992 Ls4E-16 s.00E-12 L2sE-12 6.82E-17 8.00E-14 2.00E-14 L40E-17 2.00E-12 S.OOE-13 3.41E-14 4.00E-12 LOOE-12 5/11/1992 2.38E-16 s.00E-12 L2sE-12 7.63E-17 8.00E-14 2.00E-14 3.07E-17 2.00E-12 s.OOE-13 1.27E-14 4.00E-12 LOOE-12 8/10/1992 L01E-16 S.00E-12 L2SE-12 7.07E-17 8.00E-14 2.00E-14 2.80E-17 2.00E-12 S.OOE-13 L41E-14 4.00E-12 LOOE-12 11/9/1992 S.20E-17 S.00E-12 1.2SE-12 3.6sE-17 8.00E-14 2.00E-14 L78E-17 2.00E-12 s.OOE-13 L71E-14 4.00E-12 LOOE-12 2/9/1993 2.39E-16 s.00E-12 1.2sE-12 2.97E-17 8.00E-14 2.00E-14 6.31E-17 2.00E-12 s.OOE-13 3.41E-14 4.00E-12 LOOE-12 5/10/1993 LOOE-16 S.00E-12 L2SE-12 7.11E-17 8.00E-14 2.00E-14 3.19E-17 2.00E-12 S.OOE-13 L34E-14 4.00E-12 LOOE-12 8/10/1993 L90E-16 S.00E-12 L2sE-12 LOOE-16 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 L80E-14 4.00E-12 LOOE-12 11/8/1993 LOOE-16 s.00E-12 L2sE-12 LOOE-16 8.00E-14 2.00E-14 LOOE-16 2.00E-12 s.OOE-13 L49E-14 4.00E-12 LOOE-12 2/7/1994 2.23E-16 S.00E-12 L2SE-12 LOOE-16 8.00E-14 2.00E-14 L84E-16 2.00E-12 S.OOE-13 2.19E-14 4.00E-12 LOOE-12 5/9/1994 2.16E-16 s.00E-12 L2sE-12 7.20E-17 8.00E-14 2.00E-14 9.89E-17 2.00E-12 s.OOE-13 1.37E-14 4.00E-12 LOOE-12 8/9/1994 9.29E-17 S.00E-12 L2SE-12 2.96E-16 8.00E-14 2.00E-14 3.04E-16 2.00E-12 S.OOE-13 LOOE-16 4.00E-12 LOOE-12 11/7/1994 9.21E-17 s.00E-12 L2SE-12 2.3sE-16 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 LOOE-16 4.00E-12 LOOE-12 --- Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-2U Effluent Concentration Limit = 2E-14 uCi/ml BHV-2T Effluent Concentration Limit = 9E-13 uCi/ml BHV-2R Effluent Concentration Limit = 6E-13 uCi/ml BHV-2PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 l.18E-16 9.00E-14 2.2SE-14 9.70E-17 2.00E-14 S.00E-1S 9.70E-17 9.00E-13 2.2SE-13 7.42E-1S 6.00E-13 1.S0E-13 5/9/1995 9.40E-17 9.00E-14 2.2SE-14 1.20E-16 2.00E-14 S.00E-1S 3.S0E-16 9.00E-13 2.2SE-13 3.90E-1S 6.00E-13 1.S0E-13 8/9/1995 8.90E-17 9.00E-14 2.2SE-14 9.67E-17 2.00E-14 S.00E-1S 1.3SE-16 9.00E-13 2.2SE-13 2.38E-16 6.00E-13 1.S0E-13 11/11/1995 2.83E-1S 9.00E-14 2.2SE-14 4.09E-16 2.00E-14 S.00E-1S S.23E-16 9.00E-13 2.2SE-13 6.77E-1S 6.00E-13 1.S0E-13 2/5/1996 1.7SE-1S 9.00E-14 2.2SE-14 8.66E-16 2.00E-14 S.00E-1S 4.86E-16 9.00E-13 2.2SE-13 3.S0E-1S 6.00E-13 1.S0E-13 5/6/1996 1.40E-16 9.00E-14 2.2SE-14 l.1SE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.8SE-1S 6.00E-13 1.S0E-13 8/5/1996 1.43E-16 9.00E-14 2.2SE-14 2.78E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.83E-1S 6.00E-13 1.S0E-13 11/6/1996 1.4SE-16 9.00E-14 2.2SE-14 1.S7E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.19E-14 6.00E-13 1.S0E-13 2/6/1997 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.84E-16 6.00E-13 1.S0E-13 5/5/1997 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 3.89E-1S 6.00E-13 1.S0E-13 8/11/1997 1.00E-16 9.00E-14 2.2SE-14 1.09E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.69E-1S 6.00E-13 1.S0E-13 1/5/1998 2.SSE-16 9.00E-14 2.2SE-14 1.07E-16 2.00E-14 S.00E-1S S.00E-17 9.00E-13 2.2SE-13 S.l1E-1S 6.00E-13 1.S0E-13 4/28/1998 1.2OE-16 9.00E-14 2.2SE-14 1.71E-16 2.00E-14 S.00E-1S 1.28E-16 9.00E-13 2.2SE-13 6.40E-1S 6.00E-13 1.S0E-13 7/31/1998 1.47E-16 9.00E-14 2.2SE-14 4.24E-16 2.00E-14 S.00E-1S 3.39E-16 9.00E-13 2.2SE-13 4.80E-1S 6.00E-13 1.S0E-13 9/28/1998 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 4.26E-1S 6.00E-13 1.S0E-13 12/28/1998 2.S4E-16 9.00E-14 2.2SE-14 2.1SE-16 2.00E-14 S.00E-1S 1.38E-16 9.00E-13 2.2SE-13 6.88E-1S 6.00E-13 1.S0E-13 3/29/1999 1.07E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 7.61E-1S 6.00E-13 1.S0E-13 7/3/1999 2.46E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.9SE-1S 6.00E-13 1.S0E-13 9/27/1999 2.81E-16 9.00E-14 2.2SE-14 1.41E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 7.3SE-1S 6.00E-13 1.S0E-13 12/28/1999 S.20E-16 9.00E-14 2.2SE-14 2.60E-16 2.00E-14 S.00E-1S 2.01E-16 9.00E-13 2.2SE-13 7.00E-1S 6.00E-13 1.S0E-13 3/27/2000 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 7.12E-1S 6.00E-13 1.S0E-13 6/26/2000 1.lOE-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.16E-16 9.00E-13 2.2SE-13 S.07E-1S 6.00E-13 1.S0E-13 9/26/2000 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.31E-1S 6.00E-13 1.S0E-13 12/26/2000 1.26E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 9.4SE-1S 6.00E-13 1.S0E-13 3/26/2001 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.9SE-1S 6.00E-13 1.S0E-13 7/2/2001 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.S6E-1S 6.00E-13 1.S0E-13 9/24/2001 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.16E-1S 6.00E-13 1.S0E-13 12/31/2001 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 2.20E-1S 6.00E-13 1.S0E-13 4/1/2002 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 9.9SE-1S 6.00E-13 1.S0E-13 7/1/2002 1.2SE-16 9.00E-14 2.2SE-14 1.43E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 8.2SE-1S 6.00E-13 1.S0E-13 9/30/2002 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 3.69E-1S 6.00E-13 1.S0E-13 12/30/2002 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.91E-1S 6.00E-13 1.S0E-13 3/31/2003 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.16E-1S 6.00E-13 1.S0E-13 6/30/2003 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.27E-1S 6.00E-13 1.S0E-13 9/29/2003 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 7.23E-1S 6.00E-13 1.S0E-13 12/29/2003 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 7.80E-1S 6.00E-13 1.S0E-13 3/29/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 2.04E-14 6.00E-13 1.S0E-13 6/27/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 3.09E-1S 6.00E-13 1.S0E-13 9/27/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.73E-14 6.00E-13 1.S0E-13 12/27/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.30E-14 6.00E-13 1.S0E-13 3/28/2005 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 8.88E-1S 6.00E-13 1.S0E-13 6/29/2005 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 8.8SE-1S 6.00E-13 1.S0E-13 9/26/2005 1.00E-16 9.00E-14 2.2SE-14 1.99E-16 2.00E-14 S.00E-1S 1.44E-16 9.00E-13 2.2SE-13 3.81E-14 6.00E-13 1.S0E-13 1/3/2006 1.29E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 4.08E-16 9.00E-13 2.2SE-13 6.S8E-14 6.00E-13 1.S0E-13 4/3/2006 1.02E-16 9.00E-14 2.2SE~14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.08E-14 6.00E-13 1.S0E-13 7/3/2006 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 l.10E-14 6.00E-13 1.S0E-13 10/2/2006 1.30E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.68E-14 6.00E-13 1.S0E-13 1/1/2007 1.24E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 l.38E-14 6.00E-13 1.S0E-13 4/2/2007 1.40E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.63E-14 6.00E-13 1.S0E-13 7/2/2007 1.04E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.36E-14 6.00E-13 1.S0E-13 9/30/2007 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 8.24E-1S 6.00E-13 1.S0E-13 12/31/2007 1.91E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.18E-14 6.00E-13 l.S0E-13 3/30/2008 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.49E-1S 6.00E-13 1.S0E-13 6/30/2008 1.29E-16 9.00E-14 2.2SE-l.! 1.00E:1~ 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 4.82E-1S 6.00E-13 ~ - Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-2U Effluent Concentration Limit = 2E-14 uCi/ml BHV-2T Effluent Concentration Limit = 9E-13 uCi/ml BHV-2R Effluent Concentration Limit = 6E-13 uCi/ml BHV-2PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 2.73E-16 9.00E-14 2.2sE-14 LOOE-16 2.00E-14 s.00E-1s LOOE-16 9.00E-13 2.2sE-13 8.30E-1s 6.00E-13 LsOE-13 12/31/2008 S.71E-16 9.00E-14 2.2sE-14 L61E-16 2.00E-14 S.00E-1s 1.2sE-16 9.00E-13 2.2sE-13 2.04E-14 6.00E-13 LSOE-13 3/15/2009 3.96E-16 9.00E-14 2.2sE-14 1.38E-16 2.00E-14 s.00E-1S L07E-16 9.00E-13 2.2sE-13 4.81E-1s 6.00E-13 LsOE-13 6/15/2009 L24E-17 9.00E-14 2.2sE-14 4.64E-17 2.00E-14 s.00E-1S S.l1E-17 9.00E-13 2.2sE-13 4.s8E-1s 6.00E-13 LsOE-13 9/15/2009 2.43E-16 9.00E-14 2.2sE-14 s.28E-17 2.00E-14 s.00E-1s 4.84E-17 9.00E-13 2.2sE-13 L19E-14 6.00E-13 LSOE-13 12/15/2009 S.72E-16 9.00E-14 2.2SE-14 2.94E-17 2.00E-14 s.00E-1S 2.s7E-17 9.00E-13 2.2sE-13 6.70E-1S 6.00E-13 LsOE-13 3/31/2010 S.47E-16 9.00E-14 2.2sE-14 L42E-17 2.00E-14 s.00E-1s 4.66E-17 9.00E-13 2.2SE-13 8.24E-1s 6.00E-13 LSOE-13 6/30/2010 3.58E-16 9.00E-14 2.2SE-14 6.64E-17 2.00E-14 s.00E-1S 9.90E-17 9.00E-13 2.2SE-13 2.01E-1s 6.00E-13 LSOE-13 9/30/2010 2.91E-16 9.00E-14 2.2SE-14 4.48E-17 2.00E-14 s.00E-1s S.72E-17 9.00E-13 2.2sE-13 L08E-1s 6.00E-13 LsOE-13 12/31/2010 S.73E-16 9.00E-14 2.2SE-14 7.24E-17 2.00E-14 s.00E-1S 6.76E-17 9.00E-13 2.2SE-13 L3sE-14 6.00E-13 LsOE-13 4/4/2011 3.79E-16 9.00E-14 2.2SE-14 4.01E-17 2.00E-14 s.00E-1S 9.11E-17 9.00E-13 2.2SE-13 L06E-14 6.00E-13 LsOE-13 7/4/2011 3.07E-16 9.00E-14 2.2SE-14 8.S4E-17 2.00E-14 s.00E-1S 9.21E-17 9.00E-13 2.2sE-13 7.21E-1s 6.00E-13 LsOE-13 10/3/2011 L17E-16 9.00E-14 2.2SE-14 3.04E-17 2.00E-14 s.00E-1s 2.81E-17 9.00E-13 2.2SE-13 L03E-14 6.00E-13 LsOE-13 1/3/2012 3.6sE-16 9.00E-14 2.2SE-14 2.72E-17 2.00E-14 s.00E-1s 4.54E-17 9.00E-13 2.2sE-13 Ls8E-14 6.00E-13 LsOE-13 4/3/2012 4.22E-16 9.00E-14 2.2sE-14 1.1sE-16 2.00E-14 S.00E-1s 2.77E-16 9.00E-13 2.2SE-13 Ls8E-14 6.00E-13 LSOE-13 7/2/2012 3.39E-16 9.00E-14 2.2sE-14 Ls6E-16 2.00E-14 S.00E-1s L74E-16 9.00E-13 2.2sE-13 8.60E-1s 6.00E-13 LSOE-13 10/1/2012 3.13E-16 9.00E-14 2.2SE-14 4.13E-17 2.00E-14 s.00E-1s 3.04E-17 9.00E-13 2.2sE-13 L03E-14 6.00E-13 LsOE-13 12/31/2012 2.76E-16 9.00E-14 2.2sE-14 s.41E-17 2.00E-14 s.00E-1s 7.0sE-17 9.00E-13 2.2sE-13 L48E-14 6.00E-13 LsOE-13 -E ;:: () ::l -tn s::: o +i t! ..... s::: (l) CJ s::: o () (l) "C CJ ::l s::: .2 "C co 0::: N I > J: CO N ~ I W 0 ~ 1' .... """'" • • • • - ~ • ('t') ~ I W 0 ~ ~ ~ ~ ~ • • r-, ~r===::: .p. ~ -I~ 'IIIr====:: ... ~ ~~ ::::. ~ -~ --,~ -- ~ ~~~ ~ ~ ~i"- --.k-I ~ "'~ ..... .... ~~ ::. ~- • ~ ::::::: ~ ::::::: ~ ::::;: ~ ..... ~~ !~ ~ ~ :::::::: b ...... ~ ..... ...,:::; r:::::::: ~ ~ F ~ ~ ~ ~ I W 0 ~ I~ ,. 14 ~ -= ~ ..... ;--~ "'Plif ~ ~ ~~ ~, ~~ ~ ~ ~ • ~ ,~ .. c:;:::.9 r-...... 4I~ ~ W" 'F G~-des ~ ~-des o~-des 60-deS 'F ~f:: r-~ ~ 1 so-des LO-deS 90-deS ~ ~~ f::. ~ 90-des vO-deS 0 ~ N I £O-deS "'0 co (]) ..; =-t : ~ Go-des -' t ~o-des j OO-deS <.0 N N I .... ~ ~ 1-~ ~ 66-deS E ::l S6-des ~ co c::: 1'-:: ~ ,.~ ~ ~ L6-deS t 96-deS 0 ..,......rr liJ.il1ilo. I· F=:: :::J ('t') 96-des N I E v6-deS ::l ·c ~ :s .. ~ ~ 4~ Ei2 L: • c ~ ~ • .. ~ ~ -- 0 £6-deS ..c I- G6-deS t ~6-des ro L.. ::l =-'F j :'''''lI ~ ... ~~~ ~ } ,,- 06-des --co z 6S-deS E .~ ss-des c co L.. ~. ..... . 14~ ~ .... ~ • .. -""'" ;;;;;:;a: ~ => LS-deS t 9S-deS '" • .. 9s-des 'F vs-des ~ .. "". .... r-k-. £s-des ..... .... ~ ....-; ~ =-~ ~~ • IcP ..... .. .. Gs-des ~s-des LO <.0 r--CX) ~ ~ ~ ~ I I I I W W W W 0 0 0 0 ~ ~ ~ ~ ~ (ele~s 601) 1.00E-1 1 1.00E-12 1.00E-13 (j) ro u Cf.LOOE-14 0> o --J ........... 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 9E-14 uCi/ml AlARA Goal = 2.25E-14 uCi/ml Pre 1994 MPC Limit = 5E-12uCi/ml Pre 1994 AlARA Goal = 1.25E-12 uCi/ml ~ t I ~ .. II na II \~ • l\llIo. .. ' ... " I·" I ~ .. l • \/ ~ !~ .... • ~ • 1* f~ rw\ • , \ V .. T""" N (V) -.;:t L.() <.0 ex:> ex:> ex:> ex:> ex:> ex:> I I I I I I 0.. 0.. 0.. 0.. 0.. 0.. Q) Q) Q) Q) Q) Q) CI) CI) CI) CI) CI) CI) I'-ex:> Q) ex:> ex:> ex:> I I I 0.. 0.. 0.. Q) Q) Q) CI) CI) CI) o Q) I 0.. Q) CI) U. ... T""" Q) I 0.. Q) CI) " <ill N (V) Q) Q) I I 0.. 0.. Q) Q) CI) CI) ~ L.() Q) Q) I I 0.. 0.. Q) Q) CI) CI) BHV-2 Uranium-Natural Concentrations (uCi/ml) .. 1\ 1 t t' ~W\j <.0 Q) I 0.. Q) CI) I'-ex:> Q) Q) I I 0.. 0.. Q) Q) CI) CI) Q) Q) I 0.. Q) CI) t.A_* o o I 0.. Q) CI) T""" o I 0.. Q) CI) N o I 0.. Q) CI) (V) o I 0.. Q) CI) -.;:t o I 0.. Q) CI) .... --.... 1\ I \ I\. • I T ~ L.() o I 0.. Q) CI) <.0 o I 0.. Q) CI) I'-ex:> o 0 I I 0.. 0.. Q) Q) CI) CI) 1 ~ ~ .,--.. ~ ~~ Q) o I 0.. Q) CI) ... 'I o T""" I 0.. Q) CI) ~ T""" I 0.. Q) CI) ~ N T""" I 0.. Q) CI) -E :::: o :::l -tn C o +:. cu a... .... C Q) (J c o o o M N I E :::l ";: o .c l- N > J: £II T""" T""" I UJ o o N T""" I UJ 0 ~ .. - """""'" 4 ('l) .;:t LO T""" T""" T""" I I I UJ UJ UJ 0 0 0 ~ o 0 ~ele~s 601f .. I ~~ ~k ~ ~ : ~ ~ . : 1+= f:;: ~ ~ -=:::. ~ ~ !:: ~ ~ .. ~ 4E ~~ ~ ...... -~ : -I--- ,.. ..... ~ ~~ -r ....... 'II~ ~ U I-P ~ !-~ 14 f:; ~ ~~ ~ co T""" I UJ 0 ~ T""" ~ ..~, ,~ • -~ ........ • r-.. ¥~ ::=. ..... I. ~ t-- T""" I UJ 0 ~ I-- l- I-- I- 00 T""" I UJ 0 ~ T""" G~-des ~ ~-des o~-des 60-des so-des LO-deS 90-deS 90-deS vO-deS £o-des Go-des ~o-des oo-des 66-deS S6-deS L6-deS 96-deS 96-deS v6-deS £6-deS G6-des ~6-des 06-deS 6s-des ss-des LS-deS 9S-deS 9s-des vs-des £s-des Gs-des ~s~des 1.00E-11 1.00E-12 1.00E-13 Q) ro ~.OOE-14 Q) o .....J ---- 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 9E-13 uCilml ALARA Goa! = 2.25E-13 uCi/ml BHV-2 Radium-226 Concentrations (uCi/ml) Pre 1994 MPC Limit = 2E-12uCilml Pre 1994 ALARA Goal = 5E-13 uCi/ml \ • \ \ t IV ... \l ... , .. • r~ • \ JI , -., ..... . , 4 14 ..... , 11 ~ f 1\ 1\ I ~ ...... ~ T II l.tI'J~ ~ '\ JV'lJ ¥ L.............. + VtA ~ N ex:> ex:> I I 0. 0. W W (f) (f) \. .. ('t') ~ ex:> ex:> I I 0. 0. W W (f) (f) '\j I.{) ex:> I 0. W (f) CD ex:> I 0. W (f) I'-ex:> I 0. W (f) ex:> 0) ex:> ex:> I I 0. 0. W W (f) (f) o 0) I 0. W (f) , n , '\I \ ..... I ~ ~ "I ¥ • ~ 0) I 0. W (f) N ('t') ~ 0) 0) 0) I I I 0. 0. 0. W W W (f) (f) (f) I.{) CD 0) 0) I I 0. 0. W W (f) (f) .III.. .... I'-ex:> 0) 0) I I 0. 0. W W (f) (f) 0) 0) I 0. W (f) o o I 0. W (f) ~ N ('t') o 0 0 I I I 0. 0. 0. W W W (f) (f) (f) ~ o I 0. W (f) .... 1{ I j\ I.{) o I 0. W (f) CD o I 0. W (f) A. .... ...... ... ~ . \I • I'-ex:> 0) o 0 0 I I I 0. 0. 0. W W W (f) (f) (f) o ~ I 0. W (f) ,. V ... ~ I 0. W (f) I ~ .~ II 1 N ~ I 0. W (f) 1.00E-11 1.00E-12 1.00E-13 ID ro u cr.t .OOE-14 0> o -.J ........, 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1 E-12 uCi/ml • T 1\ .... 1\ . .... I' &J{ • 7r • ~ \.... /\ft 4 / ~\ ;' .It.. ~\ /\ ~ ~ ~ ~ 1"\~ ..}¥ 't T \/ ¥)l V '¥" ~ p "r" N ("I") ""'" LO <0 "-ro 0> 0 "r" N ("I") ro ro ro ro ro ro ro ro ro 0> 0> 0> 0> I I I I I I I I I I I I I c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) I .... ""'" 0> I c.. Q) C/) BHV-2 Lead-210 Concentrations (uCi/ml) 'I /\ t • ~~ J ~ ~ t ... hN -,11. Y ... , .... 'W ... .-J "\., " \..1"" , ........ I l..r. ...... • I v'" II r ..K. ... I • 1 T 1/ , LO <0 "-ro 0> 0 "r" N ("I") ""'" LO <0 "-ro 0> 0 N 0> 0> 0> 0> 0> 0 0 0 0 0 0 0 0 0 0 "r" "r" "r" I I I I I I I I I I I I I I I I I I c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) '" TAB 3 BHV-3 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-3U Effluent Concentration Limit = 2E-14 uCi/ml BHV-3T Effluent Concentration Limit = 9E-13 uCi/ml BHV-3R Effluent Concentration Limit = 6E-13 uCi/ml BHV-3PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 L74E-1S S.00E-12 L2SE-12 9.02E-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 S.OOE-13 LS4E-14 4.00E-12 LOOE-12 12/14/1981 LS9E-1S S.00E-12 L2SE-12 S.03E-16 8.00E-14 2.00E-14 1.30E-16 2.00E-12 S.OOE-13 2.2SE-14 4.00E-12 LOOE-12 3/29/1982 3.76E-16 S.00E-12 L2SE-12 S.2SE-16 8.00E-14 2.00E-14 4.08E-16 2.00E-12 S.OOE-13 L96E-14 4.00E-12 LOOE-12 6/30/1982 3.83E-16 S.00E-12 L2SE-12 2.16E-16 8.00E-14 2.00E-14 L41E-1S 2.00E-12 S.OOE-13 2.40E-14 4.00E-12 LOOE-12 9/27/1982 S.9SE-16 S.00E-12 L2SE-12 L44E-1S 8.00E-14 2.00E-14 S.36E-16 2.00E-12 S.OOE-13 L43E-14 4.00E-12 LOOE-12 1/3/1983 2.0SE-16 S.00E-12 L2SE-12 L23E-16 8.00E-14 2.00E-14 1.10E-16 2.00E-12 S.OOE-13 3.01E-14 4.00E-12 LOOE-12 4/4/1983 LOOE-16 S.00E-12 L2SE-12 6.94E-17 8.00E-14 2.00E-14 6.11E-17 2.00E-12 S.OOE-13 1.39E-14 4.00E-12 LOOE-12 6/30/1983 3.06E-16 S.OOE-12 1.2SE-12 9.59E-17 8.00E-14 2.00E-14 2.08E-16 2.00E-12 S.OOE-13 L70E-14 4.00E-12 LOOE-12 10/3/1983 L91E-16 S.00E-12 L2SE-12 3.0SE-16 8.00E-14 2.00E-14 2.79E-16 2.00E-12 S.OOE-13 L76E-14 4.00E-12 LOOE-12 1/3/1984 3.01E-16 S.00E-12 L2SE-12 9.S1E-17 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 9.17E-1S 4.00E-12 LOOE-12 4/2/1984 8.22E-16 S.00E-12 L2SE-12 7.S2E-16 8.00E-14 2.00E-14 S.20E-17 2.00E-12 S.OOE-13 3.47E-14 4.00E-12 LOOE-12 7/2/1984 S.29E-16 S.00E-12 L2SE-12 6.18E-16 8.00E-14 2.00E-14 L40E-16 2.00E-12 S.OOE-13 1.32E-14 4.00E-12 LOOE-12 10/1/1984 L74E-16 S.00E-12 1.2SE-12 7.10E-17 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 L08E-14 4.00E-12 LOOE-12 1/2/1985 LOOE-17 S.00E-12 1.2SE-12 7.10E-17 8.00E-14 2.00E-14 7.80E-17 2.00E-12 S.OOE-13 2.73E-14 4.00E-12 LOOE-12 4/1/1985 LOOE-16 S.00E-12 L2SE-12 2.76E-16 8.00E-14 2.00E-14 4.lOE-17 2.00E-12 S.OOE-13 1.12E-14 4.00E-12 LOOE-12 7/1/1985 L04E-16 S.00E-12 1.2SE-12 LOOE-16 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 L64E-14 4.00E-12 LOOE-12 9/30/1985 LOOE-16 S.00E-12 L2SE-12 LOOE-1S 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 L73E-14 4.00E-12 LOOE-12 1/2/1986 L03E-1S S.00E-12 L2SE-12 3.17E-16 8.00E-14 2.00E-14 L2SE-16 2.00E-12 S.OOE-13 L21E-17 4.00E-12 LOOE-12 4/1/1986 8.04E-16 S.00E-12 L2SE-12 L93E-17 8.00E-14 2.00E-14 LS4E-16 2.00E-12 S.OOE-13 L69E-14 4.00E-12 LOOE-12 6/30/1986 4.29E-16 S.00E-12 L2SE-12 L77E-16 8.00E-14 2.00E-14 2.83E-16 2.00E-12 S.OOE-13 L97E-14 4.00E-12 LOOE-12 10/27/1986 6.4SE-16 S.00E-12 1.2SE-12 9.89E-17 8.00E-14 2.00E-14 4.16E-1S 2.00E-12 S.OOE-13 L64E-14 4.00E-12 LOOE-12 12/15/1986 L31E-16 S.00E-12 L2SE-12 O.OOE+OO 8.00E-14 2.00E-14 4.16E-17 2.00E-12 S.OOE-13 4.60E-1S 4.00E-12 LOOE-12 3/16/1987 2.01E-16 S.00E-12 L2SE-12 L20E-16 8.00E-14 2.00E-14 S.73E-17 2.00E-12 S.OOE-13 L60E-14 4.00E-12 LOOE-12 5/11/1987 2.16E-16 S.00E-12 L2SE-12 L96E-16 8.00E-14 2.00E-14 7.38E-17 2.00E-12 S.OOE-13 LS9E-14 4.00E-12 LOOE-12 9/9/1987 2.41E-16 S.00E-12 L2SE-12 2.18E-16 8.00E-14 2.00E-14 3.52E-17 2.00E-12 S.OOE-13 L46E-14 4.00E-12 LOOE-12 11/2/1987 2.44E-16 S.00E-12 L2SE-12 2.32E-16 8.00E-14 2.00E-14 2.37E-17 2.00E-12 S.OOE-13 2.48E-14 4.00E-12 LOOE-12 2/16/1988 8.08E-16 S.00E-12 L2SE-12 2.5SE-16 8.00E-14 2.00E-14 3.42E-16 2.00E-12 S.OOE-13 S.61E-14 4.00E-12 LOOE-12 5/18/1988 1.14E-16 S.00E-12 L2SE-12 4.14E-17 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 L20E-14 4.00E-12 LOOE-12 8/15/1988 2.08E-16 S.00E-12 L2SE-12 3.06E-16 8.00E-14 2.00E-14 3.6SE-17 2.00E-12 S.OOE-13 1.36E-14 4.00E-12 LOOE-12 11/14/1988 4.21E-16 S.00E-12 L2SE-12 2.93E-16 8.00E-14 2.00E-14 L09E-16 2.00E-12 S.OOE-13 2.48E-14 4.00E-12 LOOE-12 2/13/1989 4.4SE-16 S.00E-12 1.2SE-12 4.78E-17 8.00E-14 2.00E-14 2.47E-17 2.00E-12 S.OOE-13 3.34E-14 4.00E-12 LOOE-12 5/15/1989 LOSE-16 S.00E-12 1.2SE-12 LOOE-16 8.00E-14 2.00E-14 2.4SE-17 2.00E-12 S.OOE-13 6.56E-1S 4.00E-12 LOOE-12 8/14/1989 L31E-16 S.00E-12 L2SE-12 S.8SE-17 8.00E-14 2.00E-14 3.97E-17 2.00E-12 S.OOE-13 6.7SE-1S 4.00E-12 LOOE-12 11/13/1989 L67E-16 S.00E-12 L2SE-12 3.87E-17 8.00E-14 2.00E-14 8.03E-17 2.00E-12 S.OOE-13 L69E-14 4.00E-12 LOOE-12 2/12/1990 4.43E-16 S.00E-12 L2SE-12 LOOE-16 8.00E-14 2.00E-14 3.S0E-17 2.00E-12 S.OOE-13 2.37E-14 4.00E-12 LOOE-12 5/14/1990 3.84E-16 S.00E-12 L2SE-12 2.S4E-16 8.00E-14 2.00E-14 L02E-16 2.00E-12 S.OOE-13 L68E-14 4.00E-12 LOOE-12 8/13/1990 7.27E-17 S.00E-12 L2SE-12 2.87E-16 8.00E-14 2.00E-14 L21E-17 2.00E-12 S.OOE-13 7.86E-1S 4.00E-12 LOOE-12 11/12/1990 L84E-16 S.00E-12 1.2SE-12 1.34E-16 8.00E-14 2.00E-14 8.S3E-l,7 2.00E-12 S.OOE-13 2.01E-14 4.00E-12 LOOE-12 2/11/1991 4.66E-17 S.00E-12 L2SE-12 8.48E-16 8.00E-14 2.00E-14 L94E-17 2.00E-12 S.OOE-13 3.69E-14 4.00E-12 LOOE-12 5/13/1991 S.OSE-17 S.00E-12 L2SE-12 7.40E-17 8.00E-14 2.00E-14 7.00E-18 2.00E-12 S.OOE-13 LSOE-14 4.00E-12 LOOE-12 8/12/1991 7.14E-17 S.00E-12 L2SE-12 6.22E-17 8.00E-14 2.00E-14 7.9SE-17 2.00E-12 S.OOE-13 L77E-14 4.00E-12 LOOE-12 11/11/1991 L41E-17 S.00E-12 L2SE-12 2.19E-18 8.00E-14 2.00E-14 2.7SE-17 2.00E-12 S.OOE-13 1.18E-14 4.00E-12 LOOE-12 2/10/1992 8.12E-17 S.00E-12 L2SE-12 2.3SE-17 8.00E-14 2.00E-14 2.76E-18 2.00E-12 S.OOE-13 3.57E-14 4.00E-12 LOOE-12 5/11/1992 9.18E-17 S.00E-12 L2SE-12 S.80E-17 8.00E-14 2.00E-14 3.36E-17 2.00E-12 S.OOE-13 L28E-14 4.00E-12 LOOE-12 8/10/1992 2.00E-18 S.00E-12 1.2SE-12 4.19E-17 8.00E-14 2.00E-14 2.00E-18 2.00E-12 S.OOE-13 LS9E-14 4.00E-12 LOOE-12 11/9/1992 4.00E-17 S.00E-12 L2SE-12 2.68E-17 8.00E-14 2.00E-14 L07E-17 2.00E-12 S.OOE-13 L81E-14 4.00E-12 LOOE-12 2/9/1993 7.94E-17 S.00E-12 L2SE-12 LOOE-16 8.00E-14 2.00E-14 L09E-16 2.00E-12 S.OOE-13 2.69E-14 4.00E-12 LOOE-12 5/10/1993 L60E-17 S.00E-12 L2SE-12 S.07E-17 8.00E-14 2.00E-14 7.64E-17 2.00E-12 S.OOE-13 L26E-14 4.00E-12 LOOE-12 8/10/1993 6.00E-17 S.00E-12 L2SE-12 6.00E-18 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 LSOE-14 4.00E-12 LOOE-12 11/8/1993 LOOE-16 S.00E-12 L2SE-12 LOOE-16 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 2.10E-14 4.00E-12 LOOE-12 2/7/1994 L61E-16 S.00E-12 L2SE-12 LOOE-16 8.00E-14 2.00E-14 2.22E-16 2.00E-12 S.OOE-13 2.23E-14 4.00E-12 LOOE-12 5/9/1994 2.77E-16 S.00E-12 L2SE-12 2.80E-17 8.00E-14 2.00E-14 8.37E-18 2.00E-12 S.OOE-13 L40E-14 4.00E-12 LOOE-12 8/9/1994 7.39E-17 S.00E-12 L2SE-12 LOOE-16 8.00E-14 2.00E-14 L14E-16 2.00E-12 S.OOE-13 LOOE-16 4.00E-12 LOOE-12 11/7/1994 9.0SE-17 S.00E-12 L2SE-12 c!-i!gE-16 8.00E-14 2.00E-14 LOOE-16 2.00E-12 S.OOE-13 LOOE-16 4.00E-12 LOOE-12 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-3U Effluent Concentration Limit = 2E-14 uCi/ml BHV-3T Effluent Concentration Limit = 9E-13 uCi/ml BHV-3R Effluent Concentration Limit = 6E-13 uCi/ml BHV-3PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal= 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E~12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 7.99E-17 9.00E-14 2.2sE-14 9.60E-17 2.00E-14 s.OOE-ls 9.60E-17 9.00E-13 2.2sE-13 9.0sE-ls 6.00E-13 LsOE-13 5/9/1995 9.40E-17 9.00E-14 2.2sE-14 9.S0E-17 2.00E-14 s.OOE-ls S.60E-17 9.00E-13 2.2sE-13 2.SSE-ls 6.00E-13 LsOE-13 S/9/199S 7.30E-17 9.00E-14 2.2sE-14 9.20E-17 2.00E-14 s.OOE-ls 4.40E-17 9.00E-13 2.2sE-13 L96E-ls 6.00E-13 LsOE-13 11/11/1995 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-ls 6.5SE-17 9.00E-13 2.2sE-13 L91E-14 6.00E-13 LsOE-13 2/5/1996 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.1SE-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 LsOE-13 5/6/1996 L31E-16 9.00E-14 2.2sE-14 L39E-16 2.00E-14 s.OOE-ls LS2E-16 9.00E-13 2.2sE-13 Ls3E-14 6.00E-13 LsOE-13 S/S/1996 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 LsOE-13 11/6/1996 3.16E-16 9.00E-14 2.2sE-14 L31E-16 2.00E-14 s.OOE-ls 6.5SE-17 9.00E-13 2.2sE-13 L91E-14 6.00E-13 LsOE-13 2/6/1997 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.1SE-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 LsOE-13 5/5/1997 1.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls LS2E-16 9.00E-13 2.2sE-13 Ls3E-14 6.00E-13 LsOE-13 S/11/1997 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 LsOE-13 1/S/199S 3.16E-16 9.00E-14 2.2sE-14 L31E-16 2.00E-14 s.OOE-ls 6.5SE-17 9.00E-13 2.2sE-13 L91E-14 6.00E-13 LsOE-13 4/2S/199S 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.1SE-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 LsOE-13 7/31/199S L31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls LS2E-16 9.00E-13 2.2sE-13 Ls3E-14 6.00E-13 LsOE-13 9/2S/199S 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 L31E-14 6.00E-13 LsOE-13 12/2S/199S 3.16E-16 9.00E-14 2.2SE-14 1.31E-16 2.00E-14 s.OOE-ls 6.5SE-17 9.00E-13 2.2sE-13 L91E-14 6.00E-13 LsOE-13 3/29/1999 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.1SE-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 LsOE-13 7/3/1999 L31E-16 9.00E-14 2.2sE-14 L39E-16 2.00E-14 s.OOE-ls LS2E-16 9.00E-13 2.2sE-13 Ls3E-14 6.00E-13 LsOE-13 9/27/1999 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 L31E-14 6.00E-13 LsOE-13 12/2S/1999 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-ls 6.sSE-17 9.00E-13 2.2sE-13 L91E-14 6.00E-13 LsOE-13 3/2S/2000 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.1SE-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 LsOE-13 6/26/2000 1.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls LS2E-16 9.00E-13 2.2sE-13 Ls3E-14 6.00E-13 LsOE-13 9/26/2000 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 LsOE-13 12/26/2000 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-ls 6.sSE-17 9.00E-13 2.2sE-13 L91E-14 6.00E-13 LsOE-13 3/26/2001 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.1SE-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 LsOE-13 7/2/2001 1.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls LS2E-16 9.00E-13 2.2sE-13 Ls3E-14 6.00E-13 LsOE-13 9/24/2001 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 LsOE-13 12/31/2001 3.16E-16 9.00E-14 2.2sE-14 L31E-16 2.00E-14 s.OOE-ls 6.5SE-17 9.00E-13 2.2sE-13 L91E-14 6.00E-13 LsOE-13 4/1/2002 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.1SE-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 LsOE-13 7/1/2Q02 1.31E-16 9.00E-14 2.2sE-14 L39E-16 2.00E-14 s.OOE-ls LS2E-16 9.00E-13 2.2sE-13 Ls3E-14 6.00E-13 LsOE-13 9/30/~002 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 LsOE-13 12/30~2002 3.16E-16 9.00E-14 2.2sE-14 L31E-16 2.00E-14 s.OOE-ls 6.5SE-17 9.00E-13 2.2sE-13 L91E-14 6.00E-13 LsOE-13 3/31/~003 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.1SE-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 LsOE-13 6/30/~003 1.31E-16 9.00E-14 2.2sE-14 L39E-16 2.00E-14 s.OOE-ls LS2E-16 9.00E-13 2.2sE-13 Ls3E-14 6.00E-13 LsOE-13 9/29/~003 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 LsOE-13 12/29~2003 3.16E-16 9.00E-14 2.2sE-14 L31E-16 2.00E-14 s.OOE-ls 6.5SE-17 9.00E-13 2.2sE-13 L91E-14 6.00E-13 LsOE-13 3/29/~004 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.1SE-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 LsOE-13 6/27/~004 1.31E-16 9.00E-14 2.2sE-14 L39E-16 2.00E-14 s.OOE-ls LS2E-16 9.00E-13 2.2sE-13 Ls3E-14 6.00E-13 LsOE-13 9/27/~004 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 LsOE-13 12/27/2004 3.16E-16 9.00E-14 2.2sE-14 L31E-16 2.00E-14 s.OOE-ls 6.5SE-17 9.00E-13 2.2sE-13 L91E-14 6.00E-13 LsOE-13 3/2S/200s 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls L1SE-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 LsOE-13 6/29/~00s 1.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls LS2E-16 9.00E-13 2.2sE-13 Ls3E-14 6.00E-13 LsOE-13 9/26/~00s 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 LsOE-13 1/3/2q06 3.16E-16 9.00E-14 2.2sE-14 L31E-16 2.00E-14 s.OOE-ls 6.sSE-17 9.00E-13 2.2sE-13 L91E-14 6.00E-13 LsOE-13 4/3/2Q06 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls L1SE-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 LsOE-13 7/3/2Q06 L31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls LS2E-16 9.00E-13 2.2sE-13 Ls3E-14 6.00E-13 LsOE-13 10/2/~006 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 L31E-14 6.00E-13 LsOE-13 1/1/2Q06 3.16E-16 9.00E-14 2.2sE-14 L31E-16 2.00E-14 s.OOE-ls 6.sSE-17 9.00E-13 2.2sE-13 L91E-14 6.00E-13 LsOE-13 4/2/2Q07 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.1SE-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 LsOE-13 7/2/2Q07 1.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls LS2E-16 9.00E-13 2.2sE-13 Ls3E-14 6.00E-13 LSOE-13 9/30/~007 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 LsOE-13 12/31~2007 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-ls 6.5SE-17 9.00E-13 2.2sE-13 L91E-14 6.00E-13 LsOE-13 3/31/200S 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.1SE-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 LsOE-13 6/30/~00S L31E-16 9.00E-14 2.2SE-14 1.39E-16 2.00E-14 s.OOE-ls LS2E-16 9.00E-13 2.2sE-13 Ls3E-14 6.00E-13 LsOE-13 j Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-3U Effluent Concentration Limit = 2E-14 uCi/ml BHV-3T Effluent Concentration Limit = 9E-13 uCi/ml BHV-3R Effluent Concentration Limit = 6E-13 uCi/ml BHV-3PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2SE-13 l.31E-14 6.00E-13 l.S0E-13 12/31/2008 3.16E-16 9.00E-14 2.2SE-14 1.31E-16 2.00E-14 S.00E-1S 6.S8E-17 9.00E-13 2.2SE-13 1.91E-14 6.00E-13 l.S0E-13 3/1S/2009 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.00E-1S 1.18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 l.S0E-13 6/1S/2009 1.31E-16 9.00E-14 2.2SE-14 l.39E-16 2.00E-14 S.00E-1S 1.82E-16 9.00E-13 2.2SE-13 l.S3E-14 6.00E-13 l.S0E-13 9/1S/2009 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2SE-13 l.31E-14 6.00E-13 l.S0E-13 12/1S/2009 3.16E-16 9.00E-14 2.2SE-14 l.31E-16 2.00E-14 S.00E-1S 6.S8E-17 9.00E-13 2.2SE-13 1.91E-14 6.00E-13 l.S0E-13 3/31/2010 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.00E-1S 1.18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 l.S0E-13 6/30/2010 l.31E-16 9.00E-14 2.2SE-14 1.39E-16 2.00E-14 S.00E-1S 1.82E-16 9.00E-13 2.2SE-13 l.S3E-14 6.00E-13 l.S0E-13 9/30/2010 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2SE-13 1.31E-14 6.00E-13 l.S0E-13 12/31/2010 3.16E-16 9.00E-14 2.2SE-14 l.31E-16 2.00E-14 S.00E-1S 6.S8E-17 9.00E-13 2.2SE-13 1.91E-14 6.00E-13 l.S0E-13 4/4/2011 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.00E-1S 1.18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 l.S0E-13 7/4/2011 l.31E-16 9.00E-14 2.2SE-14 l.39E-16 2.00E-14 S.00E-1S 1.82E-16 9.00E-13 2.2SE-13 l.S3E-14 6.00E-13 l.S0E-13 10/3/2011 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2SE-13 l.31E-14 6.00E-13 l.S0E-13 1/3/2012 3.16E-16 9.00E-14 2.2SE-14 l.31E-16 2.00E-14 S.00E-1S 6.58E-17 9.00E-13 2.2SE-13 1.91E-14 6.00E-13 l.S0E-13 4/3/2012 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.00E-1S 1.18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 l.S0E-13 7/2/2012 l.31E-16 9.00E-14 2.2SE-14 l.39E-16 2.00E-14 S.00E-1S 1.82E-16 9.00E-13 2.2SE-13 l.S3E-14 6.00E-13 l.S0E-13 10/1/2012 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2SE-13 l.31E-14 6.00E-13 l.S0E-13 12/31/2012 3.16E-16 9.00E-14 2.2SE-14 1.31E-16 2.00E-14 S.00E-1S 6.58E-17 9.00E-13 2.2SE-13 1.91E-14 6.00E-13 l.S0E-13 -E :::: () :l - N "r" I W 0 ~ "r" ~=::: cry "r" I W 0 ~ ~ ~ ~ ~ ~ ~ ~ «::; ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ .... -- ..... 1 ~ ~ -=: ~ ~ :::::::.: ~ ~ ::::; r;::: .-: r.-t I· ~ D. r-..... Il- ~~ ~ .... ~ f; !. =:::: ~ ~K ~ p:. ~ r--. 'o::t "r" I W 0 ~ .... ,..~ .. ~ ", -. ~ """1IIiiiit= ~ ",-. ~ """1IIiiiiIt: ~ ",-. ~,. Iiiiiiii ~ ", -. """Iiiiiit ~ l'-' ~ ,...~ ... ~~ ~ ~ I''''' ~ ~ ,...,; l'~ ~ ,.1IIiiiiIt: .. ~ I'" ~ ,.~ ... ~ l' -. ~ ,..allliiiilt: .. ~ l'''' ~ .. 1IIiiij; ISIP_ l'''' ~ .. ~ --~ l' -. ~ _1Iiiii. -~ l1-' ~ .- ~~ -. ~ .;:;: p- ~ l1 -. ,..&;;; 111 ... ~ ~ ~ ... ~ .... '---...J 4 ..... :.~ r..-~ r--~ i1N r:;;;;;4 .. r-r-. ~ ~ r-"'~ ~ ~ ~ ~ .. ~ ) l li= 1[ ........ .-:::: Eo P"'" ~I I ir-i-"~ ~ .;:. L() (0 "r" "r" I I W W 0 0 ~ ~ (ele~s 001) l~-des !III ~ ~-des !III o~-des !III 60-deS BO-deS !III La-des 90-deS 90-des !III va-des 0 "r" Ia N I £o-des "0 ro Ie iIa (J) la-des -' t ~o-des Ia oo-des (0 N N !III I 66-deS E .~ "0 B6-deS ro 0::: II L6-des t iIa 96-des 0 ~ ... ~ cry 96-deS N I E v6-deS :::J ·c 0 ..c lA"'" £6-deS ..... l6-deS t r-1-6. L.o.. ~~ ...... ~ --~~ ~, • tt ~ ~6-des ro L... :::J 06-des ro z 6B-deS E :::J c -~. BB-des ro L... :::> 1--'+ ~ C;. LB-deS t 9B-deS ..... '"' 9B-des vB-des ~ £B-deS lB-deS ~B-des " ex) "r" "r" I I W W 0 0 ~ ~ "r" 1.00E-11 1.00E-12 1.00E-13 ".1..00E-14 Q) ro () (J) 0) o .....J -r.OOE-15 1.00E-16 1.00E-17 1.00E-18 , Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml .... l.J\ I 1 • ~ ... ..... \ ... .J.. \ I I r \ /.., l. TV \ I .... J. \ I 'J ..... ~~ ..J r 'ill I~ .ilL ...... \I , ..-N ('I') ...;:t LO (0 I""-ex::> Q) 0 ..-ex::> ex::> ex::> ex::> ex::> ex::> ex::> ex::> ex::> Q) Q) I I I I I I I I I I I 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) BHV-3 Uranium-Natural Concentrations (uCi/ml) . --- , ~ ~ .... ~~ ~ ~ ~~ ~ ~ ~ ......... ~ ~ ~ ~ ~ ...... Jf L\ r \ r \ T \ T \ r \ T \ T \ r \ r \ r \ r \ T \ r \ r \ r \ r \ r J\ J¥ ¥ ¥ ¥ ¥ ¥ ¥ ¥ ¥ ¥ ¥ ¥ ¥ ¥ ¥ ¥ ¥ I ..,. , I \I • N ('I') ...;:t LO (0 I""-ex::> Q) 0 ..-N ('I') ...;:t LO (0 I""-ex::> Q) 0 N Q) Q) Q) Q) Q) Q) Q) Q) 0 0 0 0 0 0 0 0 0 0 ..-..-..- I I I I I I I I I I I I I I I I I I I I I 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) 1.00E-11 1.00E-12 1.00E-13 .--t.OOE-14 Q) ro o CI) C> o .....J I .OOE-15 1.00E-16 1.00E-17 1.00E-18 .... '("""" co I 0.. Q) CI) \ Effluent Concentration Limit = 2E-14 uCi/ml ALARA Goal = 5E-13 uCilml Pre 1994 MPC Limit = 8E-14uCi/ml t ..... .... J ~ t ...~ n 1f\/ BHV-3 Thorium-230 Concentrations (uCi/ml) I , \ • • • •••••••••••••• .1\.I\.I\.I\.I\.I\.I\.I\.I\.I\./~/\.I\.I\.I\.I\.I\ t J~ I~ ~I ..... j 'i ..... ...... ~ .... 1¥ ~¥ V¥~¥ ~¥ ¥¥ ~¥ ~¥ ~¥ ¥¥ ~¥ ¥ ¥'¥ ¥¥ ¥¥ ~¥ ~¥ J A ..,. \l 1>It. T " " .... I I \,1 I V I I. • \I ...,. C'\I C") ~ LO CD I'---co Q') 0 '("""" C'\I C") ~ LO CD I'---co Q') 0 '("""" C'\I C") ~ LO CD I'---co Q') 0 '("""" C'\I co co co co co co co co Q') Q') Q') Q') Q') Q') Q') Q') Q') Q') 0 0 0 0 0 0 0 0 0 0 '("""" '("""" '("""" I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) OJ OJ OJ OJ OJ OJ OJ OJ CI) (f) CI) CI) CI) (f) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) (f) CI) (f) CI) CI) CI) CI) CI) CI) CI) CI) 1.00E-11 1.00E-12 1.00E-13 ~.OOE-1 4 (J) ro u (J) 0> o .....J '-f.OOE-15 1.00E-16 1.00E-17 1.00E-18 Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml t ..... T , 1 rfl ,~ ., !¥ ~/'l~ J JL. \ "" .1 ~ ~ N ("I) oo;;t LC) <0 I"-CX) CX) CX) CX) CX) CX) CX) I I I I I I I 0.. 0.. 0.. 0.. 0.. 0.. 0.. (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) (J) • 1\ 'l. ... I \I \ ""-\1 .\7. CX) CX) I 0.. (J) (J) tf (j) CX) I 0.. (J) (J) 1\ , \ \ t 'III ~~ '\ o ~ (j) (j) I I 0.. 0.. (J) (J) (J) (J) 4 ........ 1 II 1 N ("I) (j) (j) I I 0.. 0.. (J) (J) (J) (J) BHV-3 Radium-226 Concentrations (uCi/ml) \ ,. \ ~ 11' I' ..... I \1 • ~ LC) <0 (j) (j) (j) I I I 0.. 0.. 0.. (J) (J) (J) (J) (J) (J) ...... J{ "I 1\ I 1\/ I"-(j) I 0.. (J) (J) CX) (j) I 0.. (J) (J) ...... ...... 11' 11' 11' I' I I' I \1 / (j) (j) I 0.. (J) (J) o ~ o 0 I I 0.. 0.. (J) (J) (J) (J) ...... 11' 11' I' I I \/ N o I 0.. (J) (J) ("I) o I 0.. (J) (J) .... ...... ...... ...... 11' J{ 1\ 11' 11 11' I' J\ J \ J' I I' I 1\1'1 \1 II oo;;t LC) o 0 I I 0.. 0.. (J) (» (J) (J) <0 o I 0.. (» (J) I"-o I 0.. (J) (J) CX) (j) o 0 I I 0.. 0.. (J) (J) (J) (J) ...... ...... 11' 11' 11 l' J' J I \1 \1 o ~ I 0.. (J) (J) ~ I 0.. (J) (J) N ~ I 0.. (J) (J) -E :::: o :::l -tn t: o .. f! .., t: (I) o t: o o o "I("'" N I "'C C'G (I) ...J (II) >-~ OJ T""" I W 0 ~ T""" -~ .,=: N (V) T""" T""" I I W W 0 0 ~ ~ T""" T""" ~ ~ ~ ~ ~ «:; ~ tc:; ~ ~ ~ tc:: ~ tc:; ~ tc:; ~ ~ ~ tc:; ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ... ~-..... ~' 1 ~ ~ ~ ~ ~F=: ~ ~h r;::: « r.- I ·~ ~ ~ r-r.. It-.. ~'i: T .... ~ ~ 1.1:::::: ~~ ~ ~ p. ~ r-. ..q T""" I W 0 0 (ele~s 001) LO <D T""" T""" I I W W 0 0 ~ ~ T""" T""" ..... T I' T""" I W 0 ~ G~-des ~ ~-des o~-des 60-deS so-des LO-deS 90-des 90-deS Po-des £o-des Go-des ~o-des Do-des 66-deS S6-deS L6-des 96-deS 96-des P6-des £6-deS G6-des ~6-des 06-des 6S-deS ss-des LS-deS 9s-des 9s-des Ps-des £S-deS GS-deS ~s-des TAB 4 BHV-4 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-4U Effluent Concentration Limit = 2E-14 uCi/ml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB ALARAGoal= 2.ZSE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = Z.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC limit = 8E-14 uCi/ml Pre 1994 MPC Limit = ZE-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 S.20E-1S S.OOE-12 l.2SE-12 2.93E-1S 8.00E-14 2.00E-14 2.74E-1S 2.00E-12 S.OOE-13 l.84E-14 4.00E-12 l.00E-12 12/14/1981 4.S3E-1S S.00E-12 l.2SE-12 l.78E-1S 8.00E-14 2.00E-14 2.29E-1S 2.00E-12 S.OOE-13 2.S4E-14 4.00E-12 l.00E-12 3/29/1982 l.06E-1S S.00E-12 l.2SE-12 l.42E-14 8.00E-14 2.00E-14 l.07E-1S 2.00E-12 S.OOE-13 2.31E-14 4.00E-12 l.00E-12 6/30/1982 6.03E-1S S.00E-12 l.2SE-12 l.S7E-14 8.00E-14 2.00E-14 2.62E-1S 2.00E-12 S.OOE-13 2.2SE-14 4.00E-12 l.00E-12 9/27/1982 l.26E-14 S.00E-12 l.2SE-12 7.58E-16 8.00E-14 2.00E-14 S.3SE-1S 2.00E-12 S.OOE-13 2.68E-14 4.00E-12 l.00E-12 1/3/1983 4.33E-1S S.00E-12 l.2SE-12 6.52E-16 8.00E-14 2.00E-14 6.04E-16 2.00E-12 S.OOE-13 2.57E-14 4.00E-12 l.OOE-12 4/4/1983 l.2SE-1S S.00E-12 l.2SE-12 7.17E-16 8.00E-14 2.00E-14 6.76E-16 2.00E-12 S.OOE-13 2.00E-14 4.00E-12 l.OOE-12 6/30/1983 3.73E-16 S.00E-12 l.2SE-12 9.43E-16 8.00E-14 2.00E-14 4.13E-16 2.00E-12 S.OOE-13 l.20E-14 4.00E-12 l.OOE-12 10/3/1983 2.S4E-16 S.00E-12 l.2SE-12 l.SlE-16 8.00E-14 2.00E-14 2.6SE-16 2.00E-12 S.OOE-13 2.S0E-14 4.00E-12 l.OOE-12 1/3/1984 2.76E-1S S.00E-12 l.2SE-12 l.60E-16 8.00E-14 2.00E-14 l.OSE-16 2.00E-12 S.OOE-13 l.S9E-16 4.00E-12 l.OOE-12 4/2/1984 4.27E-16 S.00E-12 l.2SE-12 2.33E-16 8.00E-14 2.00E-14 6.28E-16 2.00E-12 S.00E-13 3.67E-14 4.00E-12 l.OOE-12 7/2/1984 2.S7E-1S S.00E-12 l.2SE-12 l.36E-16 8.00E-14 2.00E-14 l.l1E-16 2.00E-12 S.OOE-13 l.S8E-14 4.00E-12 l.OOE-12 10/1/1984 4.18E-16 S.OOE-12 l.2SE-12 3.S4E-16 8.00E-14 2.00E-14 l.lOE-17 2.00E-12 S.OOE-13 9.83E-1S 4.00E-12 l.OOE-12 1/2/1985 S.30E-17 S.00E-12 l.2SE-12 3.SSE-17 8.00E-14 2.00E-14 7.00E-18 2.00E-12 S.OOE-13 2.S7E-14 4.00E-12 l.OOE-12 4/1/1985 l.00E-16 S.00E-12 l.2SE-12 6.00E-16 8.00E-14 2.00E-14 4.3SE-17 2.00E-12 S.OOE-13 S.02E-1S 4.00E-12 l.OOE-12 7/1/1985 9.36E-16 S.00E-12 l.2SE-12 2.33E-16 8.00E-14 2.00E-14 2.36E-16 2.00E-12 S.OOE-13 7.48E-1S 4.00E-12 l.OOE-12 9/30/1985 l.46E-1S S.00E-12 l.2SE-12 7.69E-16 8.00E-14 2.00E-14 S.38E-16 2.00E-12 S.OOE-13 7.86E-1S 4.00E-12 l.OOE-12 1/2/1986 8.40E-1S S.00E-12 l.2SE-12 7.60E-16 8.00E-14 2.00E-14 2.99E-16 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 l.OOE-12 4/1/1986 S.79E-1S S.00E-12 l.2SE-12 S.80E-16 8.00E-14 2.00E-14 l.34E-1S 2.00E-12 S.OOE-13 l.33E-14 4.00E-12 l.OOE-12 6/30/1986 S.19E-1S S.00E-12 l.2SE-12 7.83E-16 8.00E-14 2.00E-14 2.20E-1S 2.00E-12 S.OOE-13 7.14E-16 4.00E-12 l.OOE-12 10/27/1986 4.60E-1S S.00E-12 l.2SE-12 4.67E-16 8.00E-14 2.00E-14 2.37E-1S 2.00E-12 S.OOE-13 l.13E-14 4.00E-12 l.OOE-12 12/15/1986 2.7SE-1S S.00E-12 l.2SE-12 S.90E-16 8.00E-14 2.00E-14 9.39E-16 2.00E-12 S.OOE-13 l.20E-14 4.00E-12 l.OOE-12 3/16/1987 4.64E-1S S.00E-12 l.2SE-12 l.18E-1S 8.00E-14 2.00E-14 4.97E-16 2.00E-12 S.OOE-13 S.89E-14 4.00E-12 l.OOE-12 5/11/1987 4.3SE-1S S.00E-12 l.2SE-12 l.23E-14 8.00E-14 2.00E-14 l.13E-1S 2.00E-12 S.OOE-13 2.21E-14 4.00E-12 l.OOE-12 9/9/1987 6.39E-1S S.00E-12 l.2SE-12 l.SOE-14 8.00E-14 2.00E-14 2.26E-1S 2.00E-12 S.OOE-13 l.S7E-14 4.00E-12 l.OOE-12 11/2/1987 6.72E-1S S.00E-12 l.2SE-12 4.53E-16 8.00E-14 2.00E-14 2.20E-1S 2.00E-12 S.OOE-13 2.SSE-14 4.00E-12 l.OOE-12 2/16/1988 l.91E-1S S.00E-12 l.2SE-12 l.3SE-14 8.00E-14 2.00E-14 4.42E-16 2.00E-12 S.OOE-13 4.44E-14 4.00E-12 l.OOE-12 5/18/1988 l.78E-14 S.00E-12 l.2SE-12 4.39E-14 8.00E-14 2.00E-14 4.92E-16 2.00E-12 S.OOE-13 l.38E-14 4.00E-12 l.OOE-12 8/15/1988 7.S6E-1S S.00E-12 l.2SE-12 3.31E-14 8.00E-14 2.00E-14 l.S1E-1S 2.00E-12 S.OOE-13 l.97E-14 4.00E-12 l.OOE-12 11/14/1988 l.47E-14 S.00E-12 l.2SE-12 l.S6E-1S 8.00E-14 2.00E-14 2.S7E-1S 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 l.OOE-12 2/13/1989 2.47E-1S S.00E-12 l.2SE-12 3.14E-1S 8.00E-14 2.00E-14 6.94E-16 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 l.OOE-12 5/15/1989 2.50E-16 S.00E-12 l.2SE-12 7.68E-1S 8.00E-14 2.00E-14 9.03E-16 2.00E-12 S.OOE-13 8.0SE-1S 4.00E-12 l.OOE-12 8/14/1989 6.S0E-1S S.00E-12 l.2SE-12 4.72E-1S 8.00E-14 2.00E-14 2.3SE-1S 2.00E-12 S.OOE-13 9.9SE-1S 4.00E-12 l.OOE-12 11/13/1989 9.63E-1S S.00E-12 l.2SE-12 4.0SE-1S 8.00E-14 2.00E-14 4.03E-1S 2.00E-12 S.OOE-13 l.99E-14 4.00E-12 l.OOE-12 2/12/1990 8.92E-1S S.00E-12 l.2SE-12 3.S6E-1S 8.00E-14 2.00E-14 2.89E-1S 2.00E-12 S.OOE-13 2.69E-14 4.00E-12 l.OOE-12 5/14/1990 8.90E-1S S.00E-12 l.2SE-12 3.58E-1S 8.00E-14 2.00E-14 2.33E-1S 2.00E-12 S.OOE-13 2.09E-14 4.00E-12 l.OOE-12 8/13/1990 l.92E-1S S.00E-12 l.2SE-12 l.87E-1S 8.00E-14 2.00E-14 S.06E-16 2.00E-12 S.OOE-13 8.86E-1S 4.00E-12 l.OOE-12 11/12/1990 2.91E-1S S.00E-12 l.2SE-12 2.2SE-17 8.00E-14 2.00E-14 l.08E-1S 2.00E-12 S.OOE-13 2.19E-14 4.00E-12 l.OOE-12 2/11/1991 l.67E-16 S.00E-12 l.2SE-12 7.89E-16 8.00E-14 2.00E-14 6.38E-17 2.00E-12 S.OOE-13 4.19E-14 4.00E-12 l.00E-12 5/13/1991 l.87E-16 S.00E-12 l.2SE-12 2.61E-1S 8.00E-14 2.00E-14 3.S4E-16 2.00E-12 S.OOE-13 1.40E-14 4.00E-12 l.OOE-12 8/12/1991 4.8SE-16 S.00E-12 l.2SE-12 4.38E-16 8.00E-14 2.00E-14 l.27E-16 2.00E-12 S.OOE-13 2.20E-14 4.00E-12 l.OOE-12 11/11/1991 l.77E-16 S.00E-12 l.2SE-12 l.46E-16 8.00E-14 2.00E-14 3.76E-17 2.00E-12 S.OOE-13 l.1SE-14 4.00E-12 l.OOE-12 2/10/1992 l.83E-16 S.00E-12 l.2SE-12 l.9SE-1S 8.00E-14 2.00E-14 l.33E-16 2.00E-12 S.OOE-13 3.3SE-14 4.00E-12 l.OOE-12 5/11/1992 4.40E-16 S.00E-12 l.2SE-12 2.S6E-16 8.00E-14 2.00E-14 4.04E-16 2.00E-12 S.OOE-13 l.41E-14 4.00E-12 l.OOE-12 8/10/1992 9.09E-17 S.00E-12 l.2SE-12 l.1SE-16 8.00E-14 2.00E-14 4.50E-17 2.00E-12 S.OOE-13 l.S7E-14 4.00E-12 l.OOE-12 11/9/1992 2.07E-16 S.00E-12 l.2SE-12 l.00E-16 8.00E-14 2.00E-14 3.62E-17 2.00E-12 S.OOE-13 2.24E-14 4.00E-12 l.OOE-12 2/9/1993 l.73E-16 S.00E-12 l.2SE-12 2.76E-17 8.00E-14 2.00E-14 2.89E-17 2.00E-12 S.OOE-13 3.08E-14 4.00E-12 l.OOE-12 5/10/1993 2.70E-17 S.00E-12 l.2SE-12 2.S0E-17 8.00E-14 2.00E-14 8.74E-17 2.00E-12 S.OOE-13 l.2SE-14 4.00E-12 l.OOE-12 8/10/1993 9.00E-17 S.OOE-12 l.2SE-12 l.76E-16 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 S.OOE-13 l.SOE-14 4.00E-12 l.OOE-12 11/8/1993 l.00E-16 S.00E-12 l.2SE-12 l.00E-16 8.00E-14 2.00E-14 6.00E-17 2.00E-12 S.OOE-13 l.7SE-14 4.00E-12 l.OOE-12 2/7/1994 l.10E-16 S.00E-12 l.2SE-12 3.38E-16 8.00E-14 2.00E-14 2.21E-16 2.00E-12 S.OOE-13 3.08E-14 4.00E-12 l.OOE-12 5/9/1994 3.80E-16 S.00E-12 l.2SE-12 2.82E-16 8.00E-14 2.00E-14 3.46E-16 2.00E-12 S.OOE-13 l.73E-14 4.00E-12 l.OOE-12 8/9/1994 3.8SE-16 S.00E-12 l.2SE-12 3.53E-16 8.00E-14 2.00E-14 l.00E-16 2.00E-12 S.OOE-13 l.00E-16 4.00E-12 l.OOE-12 11/7/1994 __ 6.21E-17 S.00E-12 l.2SE-12 9.70E-17 8.00E-14 2.00E-14 l.96E-16 2.00E-12 S.OOE-13 l.00E-16 4.00E-12 l.OOE-12 ------ Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-4U Effluent Concentration Limit = 2E-14 uCi/ml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 3.70E-16 9.00E-14 2.2SE-14 9.80E-17 2.00E-14 S.00E-1S 9.70E-17 9.00E-13 2.2SE-13 8.84E-1S 6.00E-13 1.S0E-13 5/9/1995 9.40E-17 9.00E-14 2.2SE-14 2.86E-16 2.00E-14 S.00E-1S 1.90E-16 9.00E-13 2.2SE-13 2.90E-1S 6.00E-13 1.S0E-13 8/9/1995 1.4SE-16 9.00E-14 2.2SE-14 2.31E-1S 2.00E-14 S.00E-1S 7.lOE-17 9.00E-13 2.2SE-13 2.70E-1S 6.00E-13 1.S0E-13 11/11/1995 1.43E-14 9.00E-14 2.2SE-14 S.70E-1S 2.00E-14 S.00E-1S 2.61E-1S 9.00E-13 2.2SE-13 S.60E-1S 6.00E-13 1.S0E-13 2/5/1996 1.19E-14 9.00E-14 2.2SE-14 3.80E-16 2.00E-14 S.00E-1S 6.lOE-1S 9.00E-13 2.2SE-13 6.48E-1S 6.00E-13 1.S0E-13 5/6/1996 4.5SE-16 9.00E-14 2.2SE-14 3.S7E-1S 2.00E-14 S.00E-1S 2.84E-16 9.00E-13 2.2SE-13 7.68E-1S 6.00E-13 1.S0E-13 8/5/1996 7.78E-16 9.00E-14 2.2SE-14 3.S1E-1S 2.00E-14 S.00E-1S 1.69E-16 9.00E-13 2.2SE-13 4.90E-1S 6.00E-13 1.S0E-13 11/6/1996 1.36E-1S 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 4.21E-16 9.00E-13 2.2SE-13 1.10E-14 6.00E-13 1.S0E-13 2/6/1997 1.00E-16 9.00E-14 2.2SE-14 1.40E-16 2.00E-14 S.00E-1S 1.03E-16 9.00E-13 2.2SE-13 6.76E-1S 6.00E-13 1.S0E-13 5/5/1997 1.00E-16 9.00E-14 2.2SE-14 4.00E-16 2.00E-14 S.00E-1S 2.24E-16 9.00E-13 2.2SE-13 4.5SE-1S 6.00E-13 1.S0E-13 8/11/1997 4.74E-16 9.00E-14 2.2SE-14 9.07E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.SSE-1S 6.00E-13 1.S0E-13 1/5/1998 8.31E-16 9.00E-14 2.2SE-14 4.82E-16 2.00E-14 S.00E-1S 1.77E-16 9.00E-13 2.2SE-13 S.28E-1S 6.00E-13 1.S0E-13 4/28/1998 3.32E-16 9.00E-14 2.2SE-14 4.43E-1S 2.00E-14 S.00E-1S 1.21E-16 9.00E-13 2.2SE-13 7.43E-1S 6.00E-13 1.S0E-13 7/31/1998 4.60E-16 9.00E-14 2.2SE-14 9.02E-16 2.00E-14 S.00E-1S 3.S4E-16 9.00E-13 2.2SE-13 6.91E-1S 6.00E-13 1.S0E-13 9/28/1998 4.08E-16 9.00E-14 2.2SE-14 4.93E-16 2.00E-14 S.00E-1S 2.S3E-16 9.00E-13 2.2SE-13 4.52E-1S 6.00E-13 1.S0E-13 12/28/1998 7.72E-16 9.00E-14 2.2SE-14 3.7SE-16 2.00E-14 S.00E-1S 3.43E-16 9.00E-13 2.2SE-13 6.73E-1S 6.00E-13 1.S0E-13 3/29/1999 S.l1E-16 9.00E-14 2.2SE-14 4.70E-16 2.00E-14 S.00E-1S 3.70E-16 9.00E-13 2.2SE-13 8.96E-1S 6.00E-13 1.S0E-13 7/3/1999 S.90E-16 9.00E-14 2.2SE-14 9.89E-16 2.00E-14 S.00E-1S 1.28E-16 9.00E-13 2.2SE-13 6.40E-1S 6.00E-13 1.S0E-13 9/27/1999 1.70E-1S 9.00E-14 2.2SE-14 7.S0E-16 2.00E-14 S.00E-1S 4.61E-16 9.00E-13 2.2SE-13 7.86E-1S 6.00E-13 1.S0E-13 12/28/1999 1.03E-1S 9.00E-14 2.2SE-14 7.S0E-16 2.00E-14 S.00E-1S 2.43E-16 9.00E-13 2.2SE-13 6.42E-1S 6.00E-13 1.S0E-13 3/27/2000 1.00E-16 9.00E-14 2.2SE-14 2.13E-16 2.00E-14 S.00E-1S 2.20E-16 9.00E-13 2.2SE-13 S.61E-1S 6.00E-13 1.S0E-13 6/26/2000 1.7SE-16 9.00E-14 2.2SE-14 3.08E-16 2.00E-14 S.00E-1S 1.11E-16 9.00E-13 2.2SE-13 3.92E-1S 6.00E-13 1.S0E-13 9/26/2000 3.6SE-16 9.00E-14 2.2SE-14 2.01E-16 2.00E-14 S.00E-1S 2.24E-16 9.00E-13 2.2SE-13 7.79E-1S 6.00E-13 1.S0E-13 12/26/2000 2.27E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 4.3SE-16 9.00E-13 2.2SE-13 8.4SE-1S 6.00E-13 1.S0E-13 3/26/2001 1.4SE-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1s 1.00E-16 9.00E-13 2.2SE-13 6.37E-1S 6.00E-13 1.S0E-13 7/2/2001 1.00E-16 9.00E-14 2.2SE-14 1.0SE-16 2.00E-14 s.00E-1S 1.00E-16 9.00E-13 2.2sE-13 6.99E-1S 6.00E-13 1.S0E-13 9/24/2001 1.91E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1s 2.01E-16 9.00E-13 2.2SE-13 8.04E-1S 6.00E-13 1.S0E-13 12/31/2001 1.38E-16 9.00E-14 2.2SE-14 2.0SE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.83E-1S 6.00E-13 1.S0E-13 4/1/2002 2.20E-16 9.00E-14 2.2SE-14 3.38E-16 2.00E-14 S.OOE-1S 1.26E-16 9.00E-13 2.2SE-13 7.48E-1S 6.00E-13 1.S0E-13 7/1/2002 1.97E-16 9.00E-14 2.2SE-14 4.lOE-16 2.00E-14 s.OOE-ls 1.00E-16 9.00E-13 2.2sE-13 7.40E-1S 6.00E-13 1.S0E-13 9/30/2002 2.30E-16 9.00E-14 2.2SE-14 2.42E-16 2.00E-14 s.00E-1S 1.S6E-16 9.00E-13 2.2SE-13 4.21E-1S 6.00E-13 1.S0E-13 12/30/2002 1.00E-16 9.00E-14 2.2SE-14 1.92E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 9.42E-1S 6.00E-13 1.S0E-13 3/31/2003 2.S0E-16 9.00E-14 2.2SE-14 1.69E-16 2.00E-14 S.00E-1S 1.29E-16 9.00E-13 2.2SE-13 4.SSE-ls 6.00E-13 1.s0E-13 6/30/2003 1.00E-16 9.00E-14 2.2SE-14 2.87E-16 2.00E-14 s.00E-1S 1.00E-16 9.00E-13 2.2SE-13 4.20E-1s 6.00E-13 1.S0E-13 9/29/2003 1.00E-16 9.00E-14 2.2sE-14 8.S3E-16 2.00E-14 s.00E-1S 3.32E-16 9.00E-13 2.2sE-13 8.69E-1S 6.00E-13 1.S0E-13 -' 12/29/2003 1.02E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.49E-1S 9.00E-13 2.2SE-13 9.4SE-1S 6.00E-13 1.s0E-13 3/29/2004 1.00E-16 9.00E-14 2.2sE-14 1.26E-16 2.00E-14 s.OOE-ls 1.00E-16 9.00E-13 2.2SE-13 2.00E-1S 6.00E-13 1.S0E-13 ! 6/27/2004 1.00E-16 9.00E-14 2.2SE-14 2.53E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2sE-13 3.23E-1S 6.00E-13 1.S0E-13 I 9/27/2004 1.00E-16 9.00E-14 2.2SE-14 1.1sE-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2SE-13 9.68E-1s 6.00E-13 1.s0E-13 12/27/2004 1.00E-16 9.00E-14 2.2SE-14 2.30E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.37E-14 6.00E-13 1.S0E-13 3/28/2005 1.00E-16 9.00E-14 2.2sE-14 2.66E-16 2.00E-14 s.00E-1S 3.1SE-16 9.00E-13 2.2SE-13 9.22E-1S 6.00E-13 1.S0E-13 6/29/2005 1.47E-16 9.00E-14 2.2SE-14 1.4SE-1S 2.00E-14 S.00E-1S 1.42E-16 9.00E-13 2.2sE-13 9.34E-1S 6.00E-13 1.S0E-13 I 9/26/2005 2.01E-16 9.00E-14 2.2sE-14 2.06E-16 2.00E-14 S.00E-1S 4.80E-16 9.00E-13 2.2sE-13 2.12E-14 6.00E-13 1.S0E-13 1/3/2006 4.S4E-16 9.00E-14 2.2SE-14 1.24E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2sE-13 3.60E-14 6.00E-13 1.S0E-13 4/3/2006 1.99E-16 9.00E-14 2.2sE-14 1.32E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 8.36E-1S 6.00E-13 1.S0E-13 7/3/2006 2.76E-16 9.00E-14 2.2SE-14 2.63E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.03E-14 6.00E-13 1.S0E-13 10/2/2006 4.97E-16 9.00E-14 2.2SE-14 2.37E-16 2.00E-14 S.00E-1s 1.00E-16 9.00E-13 2.2SE-13 1.60E-14 6.00E-13 1.S0E-13 1/1/2007 6.46E-16 9.00E-14 2.2SE-14 2.81E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2sE-13 2.lOE-14 6.00E-13 1.S0E-13 4/2/2007 7.08E-16 9.00E-14 2.2SE-14 3.20E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.S4E-14 6.00E-13 1.s0E-13 7/2/2007 9.41E-16 9.00E-14 2.2sE-14 1.46E-16 2.00E-14 S.00E-1S 1.99E-16 9.00E-13 2.2SE-13 2.S6E-14 6.00E-13 1.S0E-13 9/30/2007 3.30E-16 9.00E-14 2.2SE-14 s.sOE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2sE-13 7.S7E-1S 6.00E-13 1.s0E-13 12/31/2007 1.42 E-1s 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 s.OOE-ls 1.00E-16 9.00E-13 2.2SE-13 9.93E-1S 6.00E-13 1.S0E-13 3/31/2008 1.2SE-16 9.00E-14 2.2SE-14 7.72E-16 2.00E-14 s.00E-1S 1.00E-16 9.00E-13 2.2SE-13 4.09E-1S 6.00E-13 1.S0E-13 6/30/2008 1.28E-1s 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 3.61E-16 9.00E-13 2.2sE-13 1.18E-14 6.00E-13 1.S0E-13 -- Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-4U Effluent Concentration Limit = 2E-14 uCi/ml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB' ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/2008 2.72E-1s 9.00E-14 2.2sE-14 l.27E-1s 2.00E-14 s.00E-1s 7.66E-16 9.00E-13 2.2sE-13 1.10E-14 6.00E-13 l.sOE-13 12/31/2008 2.88E-1s 9.00E-14 2.2sE-14 1.10E-1s 2.00E-14 s.00E-1s 6.s6E-16 9.00E-13 2.2sE-13 l.38E-14 6.00E-13 l.sOE-13 3/15/2009 l.s6E-1s 9.00E-14 2.2sE-14 4.s7E-16 2.00E-14 s.00E-1s 2.99E-16 9.00E-13 2.2sE-13 4.97E-1s 6.00E-13 l.sOE-13 6/15/2009 s.67E-17 9.00E-14 2.2sE-14 2.17E-16 2.00E-14 s.00E-1s l.slE-16 9.00E-13 2.2sE-13 4.47E-1s 6.00E-13 l.sOE-13 9/15/2009 4.0sE-1s 9.00E-14 2.2sE-14 l.4sE-1s 2.00E-14 s.00E-1s 2.s2E-16 9.00E-13 2.2sE-13 l.24E-14 6.00E-13 l.sOE-13 12/15/2009 6.s0E-1s 9.00E-14 2.2sE-14 3.48E-16 2.00E-14 s.00E-1s l.33E-16 9.00E-13 2.2sE-13 7.60E-1s 6.00E-13 l.sOE-13 3/31/2010 6.01E-1s 9.00E-14 2.2sE-14 l.26E-16 2.00E-14 s.00E-1s l.34E-16 9.00E-13 2.2sE-13 l.19E-14 6.00E-13 l.sOE-13 6/30/2010 2.33E-1s 9.00E-14 2.2sE-14 7.29E-16 2.00E-14 s.00E-1s 2.66E-16 9.00E-13 2.2sE-13 3.27E-1s 6.00E-13 l.sOE-13 9/30/2010 4.77E-1s 9.00E-14 2.2sE-14 l.80E-1s 2.00E-14 s.00E-1s 8.23E-16 9.00E-13 2.2sE-13 s.l1E-1s 6.00E-13 l.sOE-13 12/31/2010 3.93E-1s 9.00E-14 2.2sE-14 3.90E-16 2.00E-14 s.00E-1s 2.56E-16 9.00E-13 2.2sE-13 l.13E-14 6.00E-13 l.sOE-13 4/4/2011 l.29E-1s 9.00E-14 2.2sE-14 l.40E-16 2.00E-14 s.00E-1s l.s8E-16 9.00E-13 2.2sE-13 l.l1E-14 6.00E-13 l.sOE-13 7/4/2011 3.30E-1s 9.00E-14 2.2sE-14 s.44E-16 2.00E-14 s.00E-1s 4.18E-16 9.00E-13 2.2sE-13 8.26E-1s 6.00E-13 l.sOE-13 10/3/2011 l.32E-1s 9.00E-14 2.2sE-14 7.89E-16 2.00E-14 s.OOE-1s l.28E-16 9.00E-13 2.2sE-13 l.18E-14 6.00E-13 l.sOE-13 1/3/2012 l.04E-1s 9.00E-14 2.2sE-14 3.2sE-16 2.00E-14 s.00E-1s 2.28E-16 9.00E-13 2.2sE-13 1.14E-14 6.00E-13 l.sOE-13 4/3/2012 2.51E-1s 9.00E-14 2.2sE-14 s.02E-16 2.00E-14 s.00E-1s 2.27E-16 9.00E-13 2.2sE-13 l.03E-14 6.00E-13 l.sOE-13 7/2/2012 2.62E-1s 9.00E-14 2.2sE-14 l.23E-1s 2.00E-14 s.00E-1s 2.97E-16 9.00E-13 2.2sE-13 9.27E-1s 6.00E-13 l.sOE-13 10/1/2012 4.0sE-1s 9.00E-14 2.2sE-14 8.33E-16 2.00E-14 s.00E-1s s.43E-16 9.00E-13 2.2sE-13 l.21E-14 6.00E-13 l.sOE-13 12/31/2012 2.32E-1s 9.00E-14 2.2sE-14 s.89E-16 2.00E-14 s.00E-1s 3.7sE-16 9.00E-13 2.2sE-13 l.s6E-14 6.00E-13 l.sOE-13 r' (Log Scale) ~ 0 0 0 0 0 0 0 0 m m m m I I I I ~ ~ ~ ~ ex> ""-l (j) 01 Sep-81 .... ~ L..Ii .,.;; Sep-82 .,--!"" ~!I - Sep-83 .... I--.. _r- Sep-84 l..o.. I~ v ..... ~ 4 [9"" Sep-85 ..... III:~ ~ ,. .. ~ I---1-- + Sep-86 Sep-87 ..... loa. ~ ...... ~ ... ........... IA ~...., c .., Sep-88 Q) :::J ~ ... --..... c· Sep-89 3 z Sep-90 Q) C .., Sep-91 ~ 'F -~r ~ .... • :::::::.. v ..... . ~ -~ ~ .-= ~ '-WI! t Sep-92 -; Sep-93 :::J" i ....... ~~ 4Irc::: ~ 0 .., Sep-94 c· 3 I Sep-95 N ~ ~ ~ ~ =-~ ...... -~ w 0 Sep-96 + Sep-97 ::0 Sep-98 Q) 0.. c· Sep-99 3 I N Sep-OO N (j) + Sep-01 Sep-02 r CD Q) Sep-03 0.. I N 0 Sep-04 Sep-05 Sep-06 Sep-07 :::z o::~ .-'" ~ 'F ~ ..... ~ ~ ~ --:~~ ..... Z~ ----.=:~ ... ... [1 ~~ .-=:: -~ .. ~ ... ~ -=::-. .. 01::: 4 ... ~ ~ ~ O~ ~ ~ ~ ~~ ·F ~ --~ ~ .. ::~ ... ~ :::.. ,:~ ~ ::"'4 ~ r- ~ ~ ~~ ~ --~ "--~ ... ~ - ~ 3 ~ ~ r-~~ ~ ~ ~ ~ ....... .. I- Sep-08 Sep-09 r7 ~ --;~ ~ :!. ~ ~I""" I Sep-10 Sep-11 Sep-12 ~-..... ~ :::::.. --~~ -=: ~ r-"I .::::::: -H ~ .-:::::= ~ +::::::: ~ ~ ~ N~ ~ ~ DI P ~ 0 0 m I ~ ~ .... ~ ..... ~ ~ ~ boA. ~ ~ ~ .... 6.6 ::::;::,~ '" ..... '- ~ ~ ..== -~ :::::. ~ .... ..-.. J ~ --..... ~ ~ :::::::: ~ :::.. :2 r ..-.: p • ~ ~ ~ t::::=-...... ~ '" ...... ~ ~ • > ---...... ~ -=t ~ ~ b6 ~ ~ ~ ~ ~ ~ , r...... 0 0 m I ~ W I 0 0 m I ~ N OJ ::I: < I ~ ;:;c D) 0-o· ::l c: (") 0- CD o o ::l (") CD ::l r+ Sil r+ o· ::l en -c: o ::::.: 3 - 1.00E-11 1.00E-12 1.00E-13 Q) ro ~.OOE-14 0> o -l -- 1.00E-15 1.00E-16 1.00E-17 .. \ ~ ~ ro I 0.. (l) CJ) Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml t t~ \ --f • .. \ \ I \/ \ \ ~ ~ I • . ~ \) ~ f .. ... l • T • ~ 1\ 1\ ~ ~ ~ J \ / ~ .. .J • N (V) -.;:t LO CD " ro Q) 0 ~ ro ro ro ro ro ro ro ro Q) Q) I I I I I I I I I I 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. (l) (l) (l) (l) (l) (l) (l) (l) (l) (l) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) 'n .... I \f1 j , , " v " N (V) -.;:t Q) Q) Q) I I I 0.. 0.. 0.. (l) (l) (l) CJ) CJ) CJ) BHV-4 Uranium-Natural Concentrations (uCi/ml) ~ .... l"f \ "7l ..... \I,. • 1\ 1'\ , \ /\ ~~ ~ ~ t ~ ~V I f '\ ..... ...... 1/ J \ ~ M ~ ~ 'w ~ • T if I • 1f /\ / • 1\ 1'+ ~t 1'? V~ j 'l V'~V\ ,~ ~ ~ LO CD " ro Q) 0 ~ N (V) -.;:t LO CD " ro Q) 0 N Q) Q) Q) Q) Q) 0 0 0 0 0 0 0 0 0 0 ~ ~ ~ I I I I I I I I I I I I I I I I I I 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. 0.. (l) (l) (l) (l) (l) (l) (l) (l) (l) (l) (l) (l) (l) (l) (l) (l) (l) (l) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) 1.00E-11 1.00E-12 1.00E-13 Q) ro ~ .OOE-14 0> o .....J .......... 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 2E-14 uCi/ml ALARA Goal = 5E-13 uCi/ml Pre 1994 MPC Limit = BE-14uCi/ml • n~ I , r1 ~~ ~~ , 1\ \. I~ II BHV-4 Thorium-230 Concentrations (uCi/ml) .i ~ I ~ ~I If \ 1 • ~ ~~, p 1 t. t ~ t ~ N 00 00 I I • -Htto " \ II \ .... \..7 I \I l.. \ I • A.. , 1\ • • .J. "" ~'" , ..... I II. 1 I \ r \ • \ \ •. * T· \ ..... *' 1 .A \ • ,. I Jl \ ./1 ~ \ ~ 19 \ 7 I J(\ ~ ~., t ~ l W\ ~ \ \ I .. ¥ , l N \1 ~ V .. I)¥ \) ~ ~ ¥ ~ ('I) """ LO CD I"-00 Q) 00 00 00 00 00 00 00 I I I I I I I \ l \ \ , ~ .. 0 ~ N Q) Q) Q) I I I ('I) """ LO CD Q) Q) Q) Q) I I I I I"-00 Q) 0 ~ N ('I) """ LO CD I"-00 Q) 0 Q) Q) Q) 0 0 0 0 0 0 0 0 0 0 ~ I I I I I I I I I I I I I I ~ I N ~ I i I c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) 1.00E-11 1.00E-12 1.00E-13 ---t.OOE-14 Q) ro () (f) C) o .....J '-1.00E-15 1.00E-16 1.00E-17 1.00E-18 Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml -Il ... 1\ l\. r. t \ .... t.~ }1' + \, \ f\ I \ 41 .... ..... 1\' '" ... ~ \. 1\1.. .. ]I ~ ."" 1\ r ~ I '. t , v . , 1 ... ~ ... ~I or-N ('i) """ LO CD f"-ro 0> 0 or-N ro ro ro ro ro ro ro ro ro 0> 0> 0> I I I I I I I I I I I I c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) \ • , , II I ~~ • 4\ '''''' T ('i) """ LO 0> 0> 0> I I I c.. c.. c.. Q) Q) Q) (f) (f) (f) BHV-4 Radium-226 Concentrations (uCi/ml) t \ • • • , y I , . 1\ 1\ 1t~ 1\ 1\ • .1\ • l... 1 \ 1\ ~~ ~I\. ,-\ ... \ ..... , 1\/\ ..... I ,~ '~'l~ ·~VJ ¥ V lJ\ml ..J ~ \.~~ JL1 ¥-.J ¥¥ CD f"-ro 0> 0 or-N ('i) """ LO CD f"-ro 0> 0 or-N 0> 0> 0> 0> 0 0 0 0 0 0 0 0 0 0 or-or-or- I I I I I I I I I I I I I I I I I c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) (f) 1.00E-11 1.00E-12 1.00E-13 (j) co ~.OOE-14 0> o .....J -- 1.00E-15 1.00E-16 1.00E-17 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994ALARA Goal = 1E-12uCi/ml ~ n • r 1\ • 1\ • ... ... l~i~ 1\ 1 • .t\~ A~\.I\ j\ 1\ , , V I\} j)~ ~ '¥' \ J \/ )J~" V ~~ lL .... ~ ~ N ("i) -.:;t LO <0 I"--CX) 0) 0 ~ N ("i) -.:;t CX) CX) CX) CX) CX) CX) CX) CX) CX) 0) 0) 0) 0) 0) I I I I I I I I I I I I I I c... c... c... c... c... c... c... c... c... c... c... c... c... c... (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) en en en en en en en en en en en en en en I BHV-4 Lead-210 Concentrations (uCi/ml) ,. J\ .t • AI ,p ... .Jt. t •....... J . _\' ... r ....... _e . ~ '\ , " , • lL. \. ... \/ . ~ . l' \ • I " ..... .... \ I ...... • \l I .&. ~ I .&. ... \r II .... I • ~ ... V V • .... LO <0 I"--CX) 0) 0 ~ N ("i) -.:;t LO <0 I"--CX) 0) 0 ~ N 0) 0) 0) 0) 0) 0 0 0 0 0 0 0 0 0 0 ~ ~ ~ I I I I I I I I I I I I I I I I I I c... c... c... c... c... c... c... c... c... c... c... c... c... c... c... c... c... c... (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) (]) en en en en en en en en en en en en en en en en en en TAB 5 BHV-5 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit = 6E-13 uCi/ml BHV-SPB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal= SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 2.44E-1S S.00E-12 L2SE-12 LS3E-1S 8.00E-14 2.00E-14 7.S4E-16 2.00E-12 S.OOE-13 L69E-14 4.00E-12 LOOE-12 12/14/1981 4.84E-1S S.00E-12 L2SE-12 2.78E-1S 8.00E-14 2.00E-14 L84E-1S 2.00E-12 S.OOE-13 LS3E-14 4.00E-12 LOOE-12 3/29/1982 L04E-1S S.00E-12 L2SE-12 2.62E-1S 8.00E-14 2.00E-14 l.11E-1S 2.00E-12 S.OOE-13 2.98E-14 4.00E-12 LOOE-12 6/30/1982 3.61E-1S S.00E-12 L2SE-12 7.61E-1S 8.00E-14 2.00E-14 L39E-1S 2.00E-12 S.OOE-13 L80E-1S 4.00E-12 LOOE-12 9/27/1982 L71E-14 S.00E-12 L2SE-12 9.46E-1S 8.00E-14 2.00E-14 3.80E-1S 2.00E-12 S.OOE-13 2.3SE-14 4.00E-12 LOOE-12 1/3/1983 L90E-14 S.00E-12 L2SE-12 S.77E-1S 8.00E-14 2.00E-14 9.34E-17 2.00E-12 S.OOE-13 4.32E-14 4.00E-12 LOOE-12 4/4/1983 S.00E-12 L2SE-12 2.33E-1S 8.00E-14 2.00E-14 S.93E-16 2.00E-12 S.OOE-13 3.01E-14 4.00E-12 LOOE-12 6/30/1983 7.62E-16 S.00E-12 L2SE-12 3.2SE-1S 8.00E-14 2.00E-14 6.28E-1S 2.00E-12 S.OOE-13 2.69E-14 4.00E-12 LOOE-12 10/3/1983 4.86E-16 S.00E-12 1.2SE-12 LlOE-1S 8.00E-14 2.00E-14 3.63E-16 2.00E-12 S.OOE-13 2.08E-14 4.00E-12 LOOE-12 1/3/1984 6.96E-1S S.00E-12 1.2SE-12 9.69E-16 8.00E-14 2.00E-14 9.60E-16 2.00E-12 S.OOE-13 L83E-14 4.00E-12 LOOE-12 4/2/1984 L64E-1S S.00E-12 1.2SE-12 L34E-1S 8.00E-14 2.00E-14 3.88E-1S 2.00E-12 S.OOE-13 4.67E-14 4.00E-12 LOOE-12 7/2/1984 l.12E-1S S.00E-12 L2SE-12 L92E-1S 8.00E-14 2.00E-14 3.31E-1S 2.00E-12 S.OOE-13 2.21E-14 4.00E-12 LOOE-12 10/1/1984 L11E-1S S.00E-12 L2SE-12 3.13E-16 8.00E-14 2.00E-14 4.21E-16 2.00E-12 S.OOE-13 LS7E-14 4.00E-12 LOOE-12 1/2/1985 7.32E-16 S.00E-12 L2SE-12 6.71E-16 8.00E-14 2.00E-14 4.94E-16 2.00E-12 S.OOE-13 2.42E-14 4.00E-12 LOOE-12 4/1/1985 2.36E-16 S.00E-12 L2SE-12 S.43E-16 8.00E-14 2.00E-14 2.71E-16 2.00E-12 S.OOE-13 L2SE-14 4.00E-12 LOOE-12 7/1/1985 7.58E-16 S.00E-12 L2SE-12 4.00E-16 8.00E-14 2.00E-14 6.90E-16 2.00E-12 S.OOE-13 2.1SE-14 4.00E-12 LOOE-12 9/30/1985 7.47E-1S S.00E-12 L2SE-12 L16E-1S 8.00E-14 2.00E-14 2.19E-1S 2.00E-12 S.OOE-13 9.20E-1S 4.00E-12 LOOE-12 1/2/1986 L7SE-14 S.00E-12 L2SE-12 7.24E-1S 8.00E-14 2.00E-14 3.83E-1S 2.00E-12 S.OOE-13 L13E-16 4.00E-12 LOOE-12 4/1/1986 2.99E-14 S.00E-12 L2SE-12 7.64E-1S 8.00E-14 2.00E-14 LS1E-14 2.00E-12 S.OOE-13 2.22E-14 4.00E-12 LOOE-12 6/30/1986 2.23E-14 S.00E-12 1.2SE-12 S.19E-1S 8.00E-14 2.00E-14 LOSE-14 2.00E-12 S.OOE-13 2.16E-14 4.00E-12 LOOE-12 10/27/1986 2.33E-14 S.00E-12 L2SE-12 7.78E-1S 8.00E-14 2.00E-14 L60E-14 2.00E-12 S.OOE-13 2.02E-14 4.00E-12 LOOE-12 12/15/1986 3.40E-14 S.00E-12 L2SE-12 S.3SE-1S 8.00E-14 2.00E-14 L47E-14 2.00E-12 S.OOE-13 2.82E-14 4.00E-12 LOOE-12 3/16/1987 2.06E-14 S.00E-12 L2SE-12 4.S0E-1S 8.00E-14 2.00E-14 6.74E-1S 2.00E-12 S.OOE-13 7.29E-14 4.00E-12 LOOE-12 5/11/1987 2.S0E-14 S.00E-12 1.2SE-12 8.54E-1S 8.00E-14 2.00E-14 8.1SE-1S 2.00E-12 S.OOE-13 3.28E-14 4.00E-12 LOOE-12 9/9/1987 2.6SE-14 S.OOE-12 1.2SE-12 6.62E-1S 8.00E-14 2.00E-14 9.34E-1S 2.00E-12 S.OOE-13 2.77E-14 4.00E-12 LOOE-12 11/2/1987 L80E-14 S.00E-12 1.2SE-12 7.09E-1S 8.00E-14 2.00E-14 7.20E-1S 2.00E-12 S.OOE-13 L77E-14 4.00E-12 LOOE-12 2/16/1988 L01E-14 S.00E-12 L2SE-12 2.98E-1S 8.00E-14 2.00E-14 3.93E-1S 2.00E-12 S.OOE-13 3.36E-14 4.00E-12 LOOE-12 5/18/1988 L78E-14 S.00E-12 L2SE-12 8.14E-1S 8.00E-14 2.00E-14 7.43E-1S 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 LOOE-12 8/15/1988 L79E-14 S.00E-12 L2SE-12 L49E-14 8.00E-14 2.00E-14 S.34E-1S 2.00E-12 S.OOE-13 2.4SE-14 4.00E-12 LOOE-12 11/14/1988 4.46E-14 S.00E-12 L2SE-12 l.39E-14 8.00E-14 2.00E-14 L17E-14 2.00E-12 S.OOE-13 3.43E-14 4.00E-12 LOOE-12 2/13/1989 L67E-14 S.00E-12 L2SE-12 S.S4E-IS 8.00E-14 2.00E-14 7.20E-1S 2.00E-12 S.OOE-13 S.02E-14 4.00E-12 LOOE-12 5/15/1989 2.03E-14 S.00E-12 L2SE-12 7.0SE-1S 8.00E-14 2.00E-14 9.S6E-16 2.00E-12 S.OOE-13 L43E-14 4.00E-12 LOOE-12 8/14/1989 2.81E-1S S.00E-12 L2SE-12 3.78E-1S 8.00E-14 2.00E-14 9.26E-1S 2.00E-12 S.OOE-13 LSOE-14 4.00E-12 LOOE-12 I 11/13/1989 S.38E-14 S.00E-12 L2SE-12 8.01E-1S 8.00E-14 2.00E-14 L81E-14 2.00E-12 S.OOE-13 4.09E-14 4.00E-12 LOOE-12 I 2/12/1990 4.48E-14 S.00E-12 L2SE-12 L48E-14 8.00E-14 2.00E-14 L28E-14 2.00E-12 S.OOE-13 3.88E-14 4.00E-12 LOOE-12 5/14/1990 2.18E-14 S.00E-12 L2SE-12 L70E-14 8.00E-14 2.00E-14 LS9E-14 2.00E-12 S.OOE-13 3.49E-14 4.00E-12 LOOE-12 8/13/1990 9.53E-1S S.00E-12 L2SE-12 L70E-14 8.00E-14 2.00E-14 3.27E-1S 2.00E-12 S.OOE-13 L27E-14 4.00E-12 LOOE-12 11/12/1990 L11E-14 S.00E-12 1.2SE-12 S.27E-1S 8.00E-14 2.00E-14 S.38E-1S 2.00E-12 S.OOE-13 LS6E-14 4.00E-12 LOOE-12 2/11/1991 6.3SE-16 S.00E-12 1.2SE-12 3.13E-16 8.00E-14 2.00E-14 2.31E-16 2.00E-12 S.OOE-13 3.89E-14 4.00E-12 LOOE-12 S/13/199l L22E-1S S.00E-12 L2SE-12 6.14E-1S 8.00E-14 2.00E-14 4.41E-1S 2.00E-12 S.OOE-13 2.S0E-14 4.00E-12 LOOE-12 8/12/1991 7.84E-16 S.00E-12 L2SE-12 L43E-1S 8.00E-14 2.00E-14 4.47E-16 2.00E-12 S.OOE-13 L84E-14 4.00E-12 LOOE-12 11/11/1991 S.37E-16 S.00E-12 L2SE-12 4.20E-16 8.00E-14 2.00E-14 l.37E-16 2.00E-12 S.OOE-13 L27E-14 4.00E-12 LOOE-12 2/10/1992 3.S4E-16 S.00E-12 L2SE-12 l.18E-16 8.00E-14 2.00E-14 4.08E-17 2.00E-12 S.OOE-13 3.69E-14 4.00E-12 LOOE-12 5/11/1992 4.71E-16 S.00E-12 L2SE-12 9.S8E-16 8.00E-14 2.00E-14 8.31E-17 2.00E-12 S.OOE-13 L43E-14 4.00E-12 LOOE-12 8/10/1992 S.32E-1S S.00E-12 L2SE-12 3.36E-16 8.00E-14 2.00E-14 L6SE-16 2.00E-12 S.OOE-13 LS9E-14 4.00E-12 LOOE-12 11/9/1992 3.66E-16 S.00E-12 L2SE-12 2.2SE-16 8.00E-14 2.00E-14 L08E-16 2.00E-12 S.OOE-13 2.24E-14 4.00E-12 LOOE-12 2/9/1993 2.0SE-16 S.00E-12 L2SE-12 9.14E-17 8.00E-14 2.00E-14 6.31E-17 2.00E-12 S.OOE-13 3.41E-14 4.00E-12 LOOE-12 5/10/1993 4.80E-16 S.00E-12 L2SE-12 8.2SE-16 8.00E-14 2.00E-14 L26E-1S 2.00E-12 S.OOE-13 L83E-14 4.00E-12 LOOE-12 8/10/1993 8.30E-16 S.00E-12 L2SE-12 L90E-16 8.00E-14 2.00E-14 2.10E-16 2.00E-12 S.OOE-13 L70E-14 4.00E-12 LOOE-12 11/8/1993 2.70E-16 S.00E-12 1.2SE-12 8.00E-17 8.00E-14 2.00E-14 7.00E-17 2.00E-12 S.OOE-13 2.34E-14 4.00E-12 LOOE-12 2/7/1994 3.18E-16 S.00E-12 L2SE-12 LOOE-16 8.00E-14 2.00E-14 S.18E-16 2.00E-12 S.OOE-13 3.64E-14 4.00E-12 LOOE-12 5/9/1994 L80E-1S S.00E-12 L2SE-12 9.78E-16 8.00E-14 2.00E-14 l.10E-1S 2.00E-12 S.OOE-13 8.30E-1S 4.00E-12 LOOE-12 8/9/1994 2.67E-1S S.00E-12 L2SE-12 L11E-1S 8.00E-14 2.00E-14 4.9SE-16 2.00E-12 S.OOE-13 LOOE-16 4.00E-12 LOOE-12 11/7/1994 9.21E-17 S.00E-12 1.2SE-12 LS9E-1S 8.00E-14 2.00E-14 L66E-1S 2.00E-12 S.OOE-13 LOOE-16 4.00E-12 LOOE-12 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit = 6E-13 uCi/ml BHV-SPB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 LS1E-1S 9.00E-14 2.2SE-14 9.S0E-16 2.00E-14 S.00E-1S 9.70E-17 9.00E-13 2.2SE-13 9.3SE-1S 6.00E-13 LSOE-13 5/9/1995 2.21E-16 9.00E-14 2.2SE-14 8.S6E-16 2.00E-14 S.00E-1S 3.06E-1S 9.00E-13 2.2SE-13 4.34E-1S 6.00E-13 LSOE-13 8/9/1995 L66E-16 9.00E-14 2.2SE-14 L67E-1S 2.00E-14 S.00E-1S 3.90E-1S 9.00E-13 2.2SE-13 S.60E-1S 6.00E-13 LSOE-13 11/11/1995 2.04E-14 9.00E-14 2.2SE-14 6.70E-1S 2.00E-14 S.00E-1S 7.6SE-1S 9.00E-13 2.2SE-13 4.47E-1S 6.00E-13 LSOE-13 2/5/1996 4.S0E-14 9.00E-14 2.2SE-14 3.58E-14 2.00E-14 S.00E-1S 2.39E-14 9.00E-13 2.2SE-13 7.30E-1S 6.00E-13 LSOE-13 5/6/1996 L76E-1S 9.00E-14 2.2SE-14 3.S7E-1S 2.00E-14 S.00E-1S 9.SSE-16 9.00E-13 2.2SE-13 7.S4E-1S 6.00E-13 LSOE-13 8/5/1996 2.37E-1S 9.00E-14 2.2SE-14 8.18E-1S 2.00E-14 S.00E-1S 7.46E-16 9.00E-13 2.2SE-13 S.7SE-1S 6.00E-13 LSOE-13 11/6/1996 3.S3E-1S 9.00E-14 2.2SE-14 S.31E-1S 2.00E-14 S.00E-1S 9.39E-16 9.00E-13 2.2SE-13 L21E-14 6.00E-13 LSOE-13 2/6/1997 L84E-16 9.00E-14 2.2SE-14 2.01E-16 2.00E-14 S.00E-1S L87E-16 9.00E-13 2.2SE-13 6.14E-1S 6.00E-13 LSOE-13 5/5/1997 S.7SE-16 9.00E-14 2.2SE-14 7.24E-16 2.00E-14 S.00E-1S 6.07E-16 9.00E-13 2.2SE-13 4.7SE-1S 6.00E-13 LSOE-13 8/11/1997 L21E-1S 9.00E-14 2.2SE-14 7.39E-16 2.00E-14 S.00E-1S S.OSE-16 9.00E-13 2.2SE-13 4.92E-1S 6.00E-13 LSOE-13 1/5/1998 9.89E-16 9.00E-14 2.2SE-14 L92E-1S 2.00E-14 S.00E-1S 6.21E-16 9.00E-13 2.2SE-13 4.68E-1S 6.00E-13 LSOE-13 4/28/1998 2.84E-1S 9.00E-14 2.2SE-14 2.38E-1S 2.00E-14 S.00E-1S L72E-1S 9.00E-13 2.2SE-13 7.3SE-1S 6.00E-13 LSOE-13 7/31/1998 7.49E-16 9.00E-14 2.2SE-14 L49E-1S 2.00E-14 S.00E-1S 8.34E-16 9.00E-13 2.2SE-13 7.01E-1S 6.00E-13 LSOE-13 9/28/1998 L07E-1S 9.00E-14 2.2SE-14 9.20E-16 2.00E-14 S.00E-1S 6.32E-16 9.00E-13 2.2SE-13 3.9SE-1S 6.00E-13 LSOE-13 12/28/1998 8.S1E-1S 9.00E-14 2.2SE-14 4.S8E-1S 2.00E-14 S.00E-1S 4.58E-1S 9.00E-13 2.2SE-13 L43E-14 6.00E-13 LSOE-13 3/29/1999 3.7SE-1S 9.00E-14 2.2SE-14 2.4SE-1S 2.00E-14 S.00E-1S 2.39E-1S 9.00E-13 2.2SE-13 8.46E-1S 6.00E-13 LSOE-13 7/3/1999 LS3E-1S 9.00E-14 2.2SE-14 8.6SE-16 2.00E-14 S.00E-1S 6.52E-16 9.00E-13 2.2SE-13 7.20E-1S 6.00E-13 LSOE-13 9/27/1999 S.83E-1S 9.00E-14 2.2SE-14 3.52E-1S 2.00E-14 S.00E-1S 2.5SE-1S 9.00E-13 2.2SE-13 8.22E-1S 6.00E-13 LSOE-13 12/28/1999 9.48E-1S 9.00E-14 2.2SE-14 6.20E-1S 2.00E-14 S.00E-1S 3.96E-1S 9.00E-13 2.2SE-13 7.S6E-1S 6.00E-13 LSOE-13 3/27/2000 2.06E-1S 9.00E-14 2.2SE-14 l.27E-1S 2.00E-14 S.00E-1S L09E-1S 9.00E-13 2.2SE-13 7.72E-1S 6.00E-13 LSOE-13 6/26/2000 LSOE-1S 9.00E-14 2.2SE-14 l.24E-1S 2.00E-14 S.00E-1S L01E-1S 9.00E-13 2.2SE-13 4.36E-1S 6.00E-13 LSOE-13 9/26/2000 L04E-1S 9.00E-14 2.2SE-14 S.4SE-16 2.00E-14 S.00E-1S 6.01E-16 9.00E-13 2.2SE-13 7.67E-1S 6.00E-13 LSOE-13 12/26/2000 L48E-1S 9.00E-14 2.2SE-14 7.S6E-16 2.00E-14 S.00E-1S 6.84E-16 9.00E-13 2.2SE-13 7.00E-1S 6.00E-13 LSOE-13 3/26/2001 4.27E-16 9.00E-14 2.2SE-14 2.19E-16 2.00E-14 S.00E-1S L89E-16 9.00E-13 2.2SE-13 6.13E-1S 6.00E-13 LSOE-13 7/2/2001 4.S2E-16 9.00E-14 2.2SE-14 4.02E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 7.48E-1S 6.00E-13 LSOE-13 9/24/2001 4.6SE-16 9.00E-14 2.2SE-14 2.06E-16 2.00E-14 S.00E-1S 2.02E-16 9.00E-13 2.2SE-13 6.98E-1S 6.00E-13 LSOE-13 12/31/2001 7.40E-16 9.00E-14 2.2SE-14 3.S1E-16 2.00E-14 S.00E-1S 3.64E-16 9.00E-13 2.2SE-13 4.72E-1S 6.00E-13 LSOE-13 4/1/2002 L26E-1S 9.00E-14 2.2SE-14 7.S3E-16 2.00E-14 S.00E-1S 7.19E-16 9.00E-13 2.2SE-13 9.6SE-1S 6.00E-13 LSOE-13 7/1/2002 L02E-1S 9.00E-14 2.2SE-14 L03E-1S 2.00E-14 S.00E-1S 3.39E-16 9.00E-13 2.2SE-13 7.20E-1S 6.00E-13 LSOE-13 9/30/2002 S.82E-16 9.00E-14 2.2SE-14 9.28E-16 2.00E-14 S.00E-1S 3.14E-16 9.00E-13 2.2SE-13 4.48E-1S 6.00E-13 LSOE-13 12/30/2002 LOOE-16 9.00E-14 2.2SE-14 7.67E-16 2.00E-14 S.00E-1S 3.48E-16 9.00E-13 2.2SE-13 9.56E-1S 6.00E-13 LSOE-13 3/31/2003 L13E-1S 9.00E-14 2.2SE-14 7.41E-16 2.00E-14 S.00E-1S 4.41E-16 9.00E-13 2.2SE-13 6.68E-1S 6.00E-13 LSOE-13 6/30/2003 4.3SE-16 9.00E-14 2.2SE-14 S.08E-16 2.00E-14 S.00E-1S 2.51E-16 9.00E-13 2.2SE-13 l.34E-1S 6.00E-13 LSOE-13 9/29/2003 LS1E-16 9.00E-14 2.2SE-14 L02E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 7.28E-1S 6.00E-13 LSOE-13 12/29/2003 LS2E-16 9.00E-14 2.2SE-14 LS4E-16 2.00E-14 S.00E-1S LS1E-16 9.00E-13 2.2SE-13 7.02E-1S 6.00E-13 LSOE-13 3/29/2004 LOOE-16 9.00E-14 2.2SE-14 L12E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 8.82E-1S 6.00E-13 LSOE-13 6/27/2004 L18E-16 9.00E-14 2.2SE-14 3.11E-16 2.00E-14 S.00E-1S L2SE-16 9.00E-13 2.2SE-13 2.47E-1S 6.00E-13 LSOE-13 9/27/2004 l.l6E-16 9.00E-14 2.2SE-14 L72E-16 2.00E-14 S.00E-1S l.l8E-16 9.00E-13 2.2SE-13 LlOE-14 6.00E-13 LSOE-13 12/27/2004 l.l4E-16 9.00E-14 2.2SE-14 L06E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 LS9E-14 6.00E-13 LSOE-13 3/28/2005 LOOE-16 9.00E-14 2.2SE-14 2.04E-16 2.00E-14 S.00E-1S L83E-16 9.00E-13 2.2SE-13 8.S7E-1S 6.00E-13 LSOE-13 6/29/2005 L83E-16 9.00E-14 2.2SE-14 3.81E-16 2.00E-14 S.00E-1S 3.09E-16 9.00E-13 2.2SE-13 L06E-14 6.00E-13 LSOE-13 9/26/2005 2.87E-16 9.00E-14 2.2SE-14 8.21E-16 2.00E-14 S.00E-1S 3.71E-14 9.00E-13 2.2SE-13 6.28E-14 6.00E-13 LSOE-13 1/3/2006 8.74E-16 9.00E-14 2.2SE-14 3.79E-16 2.00E-14 S.00E-1S l.31E-16 9.00E-13 2.2SE-13 4.32E-14 6.00E-13 LSOE-13 4/3/2006 S.22E-16 9.00E-14 2.2SE-14 6.66E-16 2.00E-14 S.00E-1S L11E-16 9.00E-13 2.2SE-13 9.34E-1S 6.00E-13 LSOE-13 7/3/2006 3.08E-16 9.00E-14 2.2SE-14 l.lOE-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 L2SE-14 6.00E-13 LSOE-13 10/2/2006 9.14E-16 9.00E-14 2.2SE-14 4.9SE-16 2.00E-14 S.00E-1S L86E-16 9.00E-13 2.2SE-13 L67E-14 6.00E-13 LSOE-13 1/1/2007 9.49E-16 9.00E-14 2.2SE-14 6.81E-16 2.00E-14 S.00E-1S 2.02E-16 9.00E-13 2.2SE-13 l.31E-14 6.00E-13 LSOE-13 4/2/2007 L08E-1S 9.00E-14 2.2SE-14 8.22E-16 2.00E-14 S.00E-1S 2.26E-16 9.00E-13 2.2SE-13 L64E-14 6.00E-13 LSOE-13 7/2/2007 LS4E-1S 9.00E-14 2.2SE-14 8.16E-16 2.00E-14 S.00E-1S 4.76E-16 9.00E-13 2.2SE-13 2.12E-14 6.00E-13 LSOE-13 9/30/2007 4.90E-16 9.00E-14 2.2SE-14 2.37E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 6.6SE-1S 6.00E-13 LSOE-13 12/31/2007 1.46E-1S 9.00E-14 2.2SE-14 S.67E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.02E-14 6.00E-13 1.S0E-13 3/31/2008 3.16E-16 9.00E-14 2.2SE-14 6.17E-16 2.00E-14 S.00E-1S 3.71E-16 9.00E-13 2.2SE-13 4.82E-1S 6.00E-13 LSOE-13 6/30/2008 3.13E-1S 9.00E-14 2.2SE-14 LSSE-1S 2.00E-14 S.00E-1S 9.27E-16 9.00E-13 2.2SE-13 7.40E-1S 6.00E-13 1.S0E-13 --.......... Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit = 6E-13 uCi/ml BHV-SPB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/30/200S 7.0SE-1S 9.00E-14 2.2SE-14 3.41E-1S 2.00E-14 S.00E-1S 2.52E-1S 9.00E-13 2.2SE-13 1.1SE-14 6.00E-13 1.S0E-13 12/31/200S 7.22E-1S 9.00E-14 2.2SE-14 2.S2E-1S 2.00E-14 S.00E-1S 3.03E-1S 9.00E-13 2.2SE-13 1.S9E-14 6.00E-13 1.S0E-13 3/15/2009 4.13E-1S 9.00E-14 2.2SE-14 1.39E-1S 2.00E-14 S.00E-1S 1.41E-1S 9.00E-13 2.2SE-13 4.66E-1S 6.00E-13 1.S0E-13 6/15/2009 2.31E-16 9.00E-14 2.2SE-14 7.79E-16 2.00E-14 S.00E-1S 6.37E-16 9.00E-13 2.2SE-13 4.1SE-1S 6.00E-13 1.S0E-13 9/15/2009 3.lOE-1S 9.00E-14 2.2SE-14 9.20E-16 2.00E-14 S.00E-1S 6.36E-16 9.00E-13 2.2SE-13 1.21E-14 6.00E-13 1.S0E-13 12/15/2009 S.77E-1S 9.00E-14 2.2SE-14 3.13E-16 2.00E-14 S.00E-1S 1.92E-16 9.00E-13 2.2SE-13 2.48E-iS 6.00E-13 1.S0E-13 3/31/2010 4.7SE-1S 9.00E-14 2.2SE-14 3.73E-16 2.00E-14 S.00E-1S 4.19E-16 9.00E-13 2.2SE-13 1.30E-14 6.00E-13 1.S0E-13 6/30/2010 4.3SE-1S 9.00E-14 2.2SE-14 7.S4E-16 2.00E-14 S.00E-1S 1.0SE-1S 9.00E-13 2.2SE-13 4.40E-1S 6.00E-13 1.S0E-13 9/30/2010 3.S7E-1S 9.00E-14 2.2SE-14 1.14E-1S 2.00E-14 S.00E-1S 7.97E-16 9.00E-13 2.2SE-13 3.7SE-1S 6.00E-13 1.S0E-13 12/31/2010 8.S2E-1S 9.00E-14 2.2SE-14 1.4SE-1S 2.00E-14 S.00E-1S 1.29E-1S 9.00E-13 2.2SE-13 1.33E-14 6.00E-13 1.S0E-13 4/4/2011 3.20E-1S 9.00E-14 2.2SE-14 S.S9E-16 2.00E-14 S.00E-1S 1.10E-1S 9.00E-13 2.2SE-13 1.4SE-14 6.00E-13 1.S0E-13 7/4/2011 6.9SE-1S 9.00E-14 2.2SE-14 2.03E-1S 2.00E-14 S.00E-1S 2.S2E-1S 9.00E-13 2.2SE-13 1.0SE-14 6.00E-13 1.S0E-13 10/3/2011 3.l1E-1S 9.00E-14 2.2SE-14 1.14E-1S 2.00E-14 S.00E-1S S.7SE-16 9.00E-13 2.2SE-13 1.41E-14 6.00E-13 1.S0E-13 1/3/2012 4.44E-1S 9.00E-14 2.2SE-14 2.14E-1S 2.00E-14 S.00E-1S 1.S3E-1S 9.00E-13 2.2SE-13 2.0SE-14 6.00E-13 1.S0E-13 4/3/2012 S.S2E-1S 9.00E-14 2.2SE-14 3.24E-1S 2.00E-14 S.00E-1S 1.79E-1S 9.00E-13 2.2SE-13 1.SSE-14 6.00E-13 1.S0E-13 7/2/2012 S.S7E-1S 9.00E-14 2.2SE-14 3.06E-1S 2.00E-14 S.00E-1S 1.21E-1S 9.00E-13 2.2SE-13 1.11E-14 6.00E-13 1.S0E-13 10/1/2012 6.73E-1S 9.00E-14 2.2SE-14 2.S9E-1S 2.00E-14 S.00E-1S 2.43E-1S 9.00E-13 2.2SE-13 1.30E-14 6.00E-13 1.S0E-13 12/31/2012 4.SOE-1S 9.00E-14 2.2SE-14 1.62E-1S 2.00E-14 S.00E-1S 1.79E-1S 9.00E-13 2.2SE-13 1.74E-14 6.00E-13 1.S0E-13 -E =:::: o :::::J - N T""" I W 0 ~ ('t') T""" I W 0 ~ T""" ..... ~ .. • ~ ~ .~ --.... 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I'-~,. ~~ .-::~ ~ .:::; ~ .. :::::: ~ ~:! ~ r-~ ~-~ ~~ --.. .~ ~ .., ;;~ ~~ JI ~ • ~ -...... ~::::: ~ ~ 14~ .... ~ ,....... ~ ~ "r" I W 0 0 (ale~s 001) l~-das ~ ~-das o~-das 60-daS SO-daS LO-daS 90-daS 90-das PO-daS =-6 ~ £O-daS lO-daS ~o-das OO-daS 66-das S6-daS L6-daS 96-daS 96-das P6-daS £6-das l6-das ~6-das 06-daS 6S-daS ss-das LS-daS 9s-das ..... 9s-das PS-daS £S-daS I ..... lS-daS I~ ~s-das LO co ~ "r" "r" "r" I I I W W W 0 0 0 ~ ~ ~ "r" TAB 6 BHV-6 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-6U Effluent Concentration Limit = 2E-14 uCi/ml BHV-6T Effluent Concentration Limit = 9E-13 uCi/ml BHV-6R Effluent Concentration Limit = 6E-13 uCi/ml BHV-6PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 12/14/1981 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 3/29/1982 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 6/30/1982 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 9/27/1982 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 1/3/1983 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 4/4/1983 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 6/30/1983 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 10/3/1983 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 1/3/1984 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 4/2/1984 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 7/2/1984 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 10/1/1984 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 1/2/1985 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 4/1/1985 S.OOE-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 7/1/1985 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 9/30/1985 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 1/2/1986 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 4/1/1986 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 6/30/1986 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 10/27/1986 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 12/15/1986 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 3/16/1987 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 5/11/1987 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 9/9/1987 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/2/1987 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/16/1988 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 5/18/1988 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/15/1988 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/14/1988 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/13/1989 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 5/15/1989 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/14/1989 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/13/1989 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/12/1990 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 5/14/1990 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/13/1990 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/12/1990 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/11/1991 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 5/13/1991 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/12/1991 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/11/1991 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/10/1992 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 5/11/1992 . S.OOE-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/10/1992 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/9/1992 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/9/1993 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 5/10/1993 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/10/1993 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/8/1993 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 2/7/1994 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 5/9/1994 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 8/9/1994 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 11/7/1994 S.00E-12 1.2SE-12 8.00E-14 2.00E-14 2.00E-12 S.OOE-13 4.00E-12 1.00E-12 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-6U Effluent Concentration Limit = 2E-14 uCi/ml BHV-6T Effluent Concentration Limit = 9E-13 uCi/ml BHV-6R Effluent Concentration Limit = 6E-13 uCi/ml BHV-6PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 2/7/1995 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 5/9/1995 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 8/9/1995 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 11/11/1995 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 2/5/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 5/6/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 8/5/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 11/6/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 2/6/1997 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 5/5/1997 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 8/11/1997 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 1/5/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 4/28/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 7/31/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 9/28/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 12/28/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 3/29/1999 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 7/3/1999 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 LSOE-13 9/27/1999 3.03E-1S 9.00E-14 2.2SE-14 l.37E-1S 2.00E-14 S.00E-1S 8.72E-16 9.00E-13 2.2SE-13 7.SSE-1S 6.00E-13 LSOE-13 12/28/1999 S.01E-1S 9.00E-14 2.2SE-14 2.89E-1S 2.00E-14 S.00E-1S 1.31E-1S 9.00E-13 2.2SE-13 8.10E-1S 6.00E-13 LSOE-13 3/30/2000 7.46E-16 9.00E-14 2.2SE-14 S.2SE-16 2.00E-14 S.00E-1S 3.00E-16 9.00E-13 2.2SE-13 7.83E-1S 6.00E-13 LSOE-13 6/26/2000 S.40E-16 9.00E-14 2.2SE-14 3.53E-16 2.00E-14 S.00E-1S 6.11E-16 9.00E-13 2.2SE-13 4.83E-1S 6.00E-13 LSOE-13 9/25/2000 3.7SE-16 9.00E-14 2.2SE-14 2.23E-16 2.00E-14 S.00E-1S L91E-16 9.00E-13 2.2SE-13 6.41E-1S 6.00E-13 LSOE-13 12/26/2000 S.21E-16 9.00E-14 2.2SE-14 3.39E-16 2.00E-14 S.00E-1S 3.28E-17 9.00E-13 2.2SE-13 8.57E-1S 6.00E-13 LSOE-13 3/26/2001 L42E-16 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 6.1SE-1S 6.00E-13 LSOE-13 7/2/2001 L81E-16 9.00E-14 2.2SE-14 L66E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 6.9SE-1S 6.00E-13 LSOE-13 9/24/2001 3.08E-16 9.00E-14 2.2SE-14 L01E-16 2.00E-14 S.00E-1S L77E-16 9.00E-13 2.2SE-13 8.S9E-1S 6.00E-13 LSOE-13 12/31/2001 3.31E-16 9.00E-14 2.2SE-14 L2SE-16 2.00E-14 S.00E-1S L09E-16 9.00E-13 2.2SE-13 3.14E-1S 6.00E-13 LSOE-13 4/1/2002 4.77E-16 9.00E-14 . 2.2SE-14 2.94E-16 2.00E-14 S.00E-1S L96E-16 9.00E-13 2.2SE-13 8.61E-1S 6.00E-13 LSOE-13 , 7/1/2002 3.68E-16 9.00E-14 2.2SE-14 4.41E-16 2.00E-14 S.00E-1S L76E-16 9.00E-13 2.2SE-13 8.20E-1S 6.00E-13 LSOE-13 9/30/2002 3.67E-16 9.00E-14 2.2SE-14 S.60E-16 2.00E-14 S.00E-1S L80E-16 9.00E-13 2.2SE-13 S.5SE-1S 6.00E-13 LSOE-13 i 12/30/2002 LOOE-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S L67E-16 9.00E-13 2.2SE-13 l.3SE-14 6.00E-13 LSOE-13 3/31/2003 L98E-16 9.00E-14 2.2SE-14 L68E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 7.77E-1S 6.00E-13 LSOE-13 6/30/2003 l.18E-16 9.00E-14 2.2SE-14 l.1SE-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 S.92E-1S 6.00E-13 LSOE-13 9/29/2003 1.00E-16 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 8.30E-1S 6.00E-13 LSOE-13 12/29/2003 LOOE-16 9.00E-14 2.2SE-14 l.36E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 6.66E-1S 6.00E-13 1.S0E-13 3/29/2004 LOOE-16 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 8.17E-1S 6.00E-13 LSOE-13 6/27/2004 LOOE-16 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 3.SSE-1S 6.00E-13 LSOE-13 9/27/2004 LOOE-16 9.00E-14 2.2SE-14 l.38E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 L22E-14 6.00E-13 LSOE-13 12/27/2004 LOSE-16 9.00E-14 2.2SE-14 L72E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 LS2E-14 6.00E-13 LSOE-13 3/28/2005 LOOE-16 9.00E-14 2.2SE-14 LOOE-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 9.34E-1S 6.00E-13 LSOE-13 6/29/2005 L28E-16 9.00E-14 2.2SE-14 L01E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 9.8SE-1S 6.00E-13 LSOE-13 9/26/2005 L98E-16 9.00E-14 2.2SE-14 S.98E-16 2.00E-14 S.00E-1S 3.SSE-16 9.00E-13 2.2SE-13 L71E-14 6.00E-13 LSOE-13 1/3/2006 7.67E-16 9.00E-14 2.2SE-14 2.88E-16 2.00E-14 S.00E-1S 3.60E-1S 9.00E-13 2.2SE-13 4.8SE-14 6.00E-13 LSOE-13 4/3/2006 2.92E-16 9.00E-14 2.2SE-14 2.00E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 L11E-14 6.00E-13 LSOE-13 7/3/2006 3.2SE-16 9.00E-14 2.2SE-14 2.36E-16 2.00E-14 S.00E-1S L08E-16 9.00E-13 2.2SE-13 l.10E-14 6.00E-13 LSOE-13 10/2/2006 S.03E-16 9.00E-14 2.2SE-14 L49E-16 2.00E-14 S.00E-1S l.19E-16 9.00E-13 2.2SE-13 2.13E-1S 6.00E-13 LSOE-13 1/1/2007 8.31E-16 9.00E-14 2.2SE-14 2.49E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 L70E-14 6.00E-13 LSOE-13 4/2/2007 S.36E-16 9.00E-14 2.2SE-14 3.1SE-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 L43E-14 6.00E-13 LSOE-13 7/2/2007 L08E-1S 9.00E-14 2.2SE-14 2.18E-16 2.00E-14 S.00E-1S LS4E-16 9.00E-13 2.2SE-13 2.04E-14 6.00E-13 LSOE-13 9/30/2007 3.92E-16 9.00E-14 2.2SE-14 L02E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 6.38E-1S 6.00E-13 LSOE-13 12/31/2007 2.92E-1S 9.00E-14 2.2SE-14 LSSE-1S 2.00E-14 S.00E-1S 3.16E-16 9.00E-13 2.2SE-13 9.19E-1S 6.00E-13 LSOE-13 3/31/2008 4.34E-16 9.00E-14 2.2SE-14 3.S1E-16 2.00E-14 S.00E-1S LOOE-16 9.00E-13 2.2SE-13 S.99E-1S 6.00E-13 LSOE-13 6/3102008 L88E-1S 9.00E-14 2.2SE-14 9.00E-16 2.00E-14 S.00E-1S 4.04E-16 9.00E-13 2.2SE-13 7.41E-1S 6.00E-13 LSOE-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-6U Effluent Concentration Limit = 2E-14 uCi/ml BHV-6T Effluent Concentration Limit = 9E-13 uCi/ml BHV-6R Effluent Concentration Limit = 6E-13 uCi/ml BHV-6PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA 9/30/2008 4.82E-1s 9.00E-14 2.2sE-14 2.lOE-1s 2.00E-14 s.00E-1s l.27E-1s 9.00E-13 2.2sE-13 l.00E-14 6.00E-13 l.sOE-13 12/31/2008 4.80E-1s 9.00E-14 2.2SE-14 l.70E-1s 2.00E-14 s.00E-1s l.2sE-1s 9.00E-13 2.2sE-13 l.49E-14 6.00E-13 l.sOE-13 3/15/2009 2.77E-1s 9.00E-14 2.2sE-14 l.01E-1s 2.00E-14 s.00E-1s 7.82E-16 9.00E-13 2.2SE-13 6.46E-1s 6.00E-13 l.sOE-13 6/15/2009 l.41E-16 9.00E-14 2.2sE-14 2.67E-16 2.00E-14 s.00E-1s l.81E-16 9.00E-13 2.2sE-13 s.76E-1s 6.00E-13 l.sOE-13 9/15/2009 4.87E-1s 9.00E-14 2.2sE-14 4.32E-16 2.00E-14 s.00E-1s 2.23E-16 9.00E-13 2.2sE-13 8.98E-1s 6.00E-13 l.sOE-13 12/15/2009 9.24E-1s 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.00E-1s l.lsE-16 9.00E-13 2.2sE-13 6.44E-1s 6.00E-13 l.sOE-13 3/31/2010 9.63E-1s 9.00E-14 2.2sE-14 l.82E-16 2.00E-14 s.00E-1s 2.06E-16 9.00E-13 2.2sE-13 l.37E-14 6.00E-13 l.sOE-13 6/30/20io 3.62E-1s 9.00E-14 2.2sE-14 3.94E-16 2.00E-14 s.00E-1s 4.89E-16 9.00E-13 2.2sE-13 4.30E-1s 6.00E-13 l.sOE-13 9/30/2010 s.42E-1s 9.00E-14 2.2sE-14 l.08E-1s 2.00E-14 s.00E-1s s.68E-16 9.00E-13 2.2sE-13 3.98E-1s 6.00E-13 l.sOE-13 12/31/2010 l.24E-14 9.00E-14 2.2sE-14 l.21E-1s 2.00E-14 s.00E-1s l.00E-1s 9.00E-13 2.2sE-13 l.s3E-14 6.00E-13 l.sOE-13 4/4/2011 2.70E-1s 9.00E-14 2.2sE-14 4.62E-16 2.00E-14 s.00E-1s 6.s1E-16 9.00E-13 2.2sE-13 l.29E-14 6.00E-13 l.sOE-13 7/4/2011 3.01E-1s 9.00E-14 2.2sE-14 7.07E-16 2.00E-14 s.00E-1s s.7sE-16 9.00E-13 2.2sE-13 7.97E-1s 6.00E-13 l.sOE-13 10/3/2011 2.0sE-1s 9.00E-14 2.2sE-14 6.12E-16 2.00E-14 s.00E-1s l.88E-16 9.00E-13 2.2sE-13 9.93E-1s 6.00E-13 l.sOE-13 1/3/2012 3.14E-1s 9.00E-14 2.2sE-14 l.09E-1s 2.00E-14 s.00E-1s 7.6sE-16 9.00E-13 2.2sE-13 l.89E-14 6.00E-13 l.sOE-13 4/3/2012 4.41E-1s 9.00E-14 2.2sE-14 l.82E-1s 2.00E-14 s.00E-1s 4.00E-16 9.00E-13 2.2sE-13 l.sOE-14 6.00E-13 l.sOE-13 7/2/2012 6.42E-1s 9.00E-14 2.2sE-14 2.2sE-1s 2.00E-14 s.00E-1s s.l1E-16 9.00E-13 2.2sE-13 9.s4E-1s 6.00E-13 l.sOE-13 10/1/2012 6.63E-1s 9.00E-14 2.2sE-14 l.31E-1s 2.00E-14 s.00E-1s l.22E-1s 9.00E-13 2.2sE-13 l.34E-14 6.00E-13 l.sOE-13 12/31/2012 3.83E-1s 9.00E-14 2.2sE-14 l.18E-1s 2.00E-14 s.00E-1s 9.30E-16 9.00E-13 2.2sE-13 l.60E-14 6.00E-13 l.sOE-13 ........ -E :'::::: o :l -tn s:::: o +i CG '-.... s:::: CI) (.) s:::: o o CI) "'C (.) :l s:::: o "'C CG 0:: CD ::> ::I: m N T""" I W T""" 1"'== < x ~ .-=:I ~ O~= --t r-~ ..: ~ ~: ~p ~~ • ? ~ " 61~ ~ ~. !... ~: ;r 41 ~~ ~ i'r 1-'" ~~ ~ ~~ ~. 1-'" f::P4 ~ ~)~ N~ .,A. ~ ~ ~ • ~ LO T""" I W ~~~ ~~ ~ ~~ ... ~ I.~ N,.,.. ~4 ;;: F-I~ .. ~ i'-~ ~r'4l .-~ 11 ~ [J ill ... !§': ~. ti ~ ~ .~ .,.. I"'"' ~ ~ ~ ~ ~ ~ ~ r ~ ~ CD T""" I W I t:::1.6 ~ CX) T""" I W ~ ~Oll£IO ~ 900l10£/6 900l19l16 o T""" N I "'0 en Q) .....J lOO(;10£/6 t CD N N 666 ~/LlI6.~ "'0 en c::: t 966~/9/9 0 ('I') C)I E ::J ·c o ..c £66~/O~/8+ ~ ::J 066 ~/£ ~/9~ E .2 c ~ ::> L96~/6/6 t v96~H/O~ ~96 ~/9l16 1.00E-11 1.00E-12 1.00E-13 Q) ro ~ .OOE-14 0> o .....J --- 1.00E-15 1.00E-16 1.00E-17 ~ 00 0> ~ -00 N -0> Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = 5E-12uCi/ml Pre 1994ALARA Goal = 1.2SE-12 uCi/ml ~ r--. 0 00 00 0> 0> 0> 0> ~ ~ ~ ---~ 0> ("t) - - ~ 0 0> -00 ("t) 0> 0> ~ -0 ~ -00 BHV-6 Uranium-Natural Concentrations (uCi/ml) f -I \ 11 'P'""Ir " . \ ~ I \ • \ .... ..t .. T J ~ ~ T • ~ n 1 ,I , •• ..... \1 V Vl lit \ r J ~ ., JI~ I 16 .. \ r \ ~ 1" 'J! 'A .... 1 ~ I CD 0> N L!) 00 ~ 0> 0> 0 0 0 ~ 0> 0> 0 0 0 0 ~ ~ N N N N --- - --L!) r--. 0 <0 0 ("t) -N ("t) N ("t) -00 -- --0 0> 0> 0> 0> 1.00E-11 1.00E-12 1.00E-13 Q) ro u ~.OOE-14 C) o .....J '-"" 1.00E-15 1.00E-16 1.00E-17 ~ co (j) ~ -co N -(j) Effluent Concentration'Limit = 2E-14 uCi/ml ALARA Goal = 5E-13 uCi/ml Pre 1994 MPC Limit = SE-14uCi/ml -----_._._-------- ~ J'-. co co (j) (j) ~ ~ - - ~ (j) 0 -(j) ~ o (j) (j) ~ -("I) ~ 00 ("I) (j) (j) ~ -o ~ -co , , \ BHV-6 Thorium-230 Concentrations (uCi/ml) CD (j) (j) ~ -L() -co ]( J (j) (j) (j) ~ -J'-. N -(j) ... ,. 'Ir "\ 6' ~. '" . \. ... \t\ T \ ~n \JJ uAJ TV ~ o o ~ o ("I) -(j) o o ~ CD N -(j) I II • • • /\ ~ l~ , I )PlIIL I II ~ • .L • \/\ T •• 1 o o N -o ("I) -(j) • ~ o ~ ("I) -o 1.00E-11 1.00E-12 1.00E-13 Q) ro ~ .OOE-14 0) o ---1 -- 1.00E-15 1.00E-16 1.00E-17 "t'"" ex:> 0> "t'"" co N -0> Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml ~ I"--ex:> ex:> 0> 0> "t'"" "t'"" --"t'"" 0> --0 0> o 0> 0> "t'"" -('I') "t'"" -ex:> ('I') 0> 0> "t'"" -o "t'"" -ex:> \ • \ , BHV-6 Radium-226 Concentrations (uCi/ml) CD 0> 0> "t'"" -L.() -ex:> ~ 0> 0> 0> "t'"" -I"--N -0> ..... ]f 1\ Jl \ t .... 'j[\ , , \I , o o ~ o ('I') -0> ~ J o o ~ CD ~ 0> ~ ..I.. .T A ~V o o ~ o ('I') -0> ... ~ . .1-' 1\ ~ T \".. T \ lr I \ I ..... ,.1 V ." .. "t'"" o ~ ('I') -o 1.00E-1 1 1.00E-12 1.00E-13 (i) ro ~.OOE-14 0) o .....J --- 1.00E-15 1.00E-16 1.00E-17 -or- CX) Q) -or--CX) N -Q) Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1 E-12 uCi/m I ~ I'-- CX) CX) Q) Q) -or--or-- - -or-Q) --0 Q) -or- o Q) Q) -or--('t) -or--CX) ('t) Q) Q) -or--o -or--CX) I I I BHV-6 Lead-210 Concentrations (uCi/ml) CD Q) Q) -or--LO -CX) Q) Q) Q) -or--I'--N -Q) ~ \_..,..\' \l V'W' v ~ \ I ..... 'W' " .I. o o ~ o ('t) -Q) T 1\ 1\ Al l. \ \I • o o N -<0 N -Q) .... M -~ "Y II J J.. t. r.t N .., -, o o ~ o ('t) -Q) 'W' \ I ...... .... -or-o N -('t) -o ATTACHMENT C BHV AIR SAMPLING LABORATORY RESULTS AND QAlQC EN:RGY www.energylab.com < ~~':!B'.~l"" :}:: ... .:.>".~;;~."' .. ''>.~~,,''''.' _."' __ ', .. , ," ." ',' . .• . ~, 'o/.J.ff~lM:~t~~I'I~:"472~p71'. -Billings, MT 800 .. 7~5 .. 4489 • Casper, WY 888 .. 235 .. 0515 LABORATORIES Analytical ExcsJISlll:B. Sines 1852 Uleft~;'WY~lu .. §<a§·"7n~ -ijapip City,SD 888-672-1225 • CoUege Station, TX 888 .. 690 .. 2218 November 10,2012 Energy Fuels Resources (USA) Inc 225 Union Blvd Ste 600 Lakewood, CO 80228-1826 Workorder No.: C12100160 ANALYTICAL SUMMARY REPORT Project Name: 3rd Quarter Air 2012 Energy Laboratories, Inc. Casper WY received the following 6 samples for Energy Fuels Resources (USA) Inc on 10/3/2012 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C12100160-001 BHV-1 10/01/12 00:00 10/03/12 Filter Composite of two or more samples Metals, Total Digestion, Total Metals Lead 210 Radium 226 Thorium, Isotopic C12100160-002 BHV-2 10/01/12 00:00 10/03/12 Filter Same As Above C12100160-003 BHV-4 10/01/12 00:00 10/03/12 Filter Same As Above C12100160-004 BHV-5 10/01/12 00:00 10/03/12 Filter Same As Above C12100160-005 BHV-6 10/01/12 00 :00 10/03/12 Filter Same As Above C12100160-006 Blank 10/01/12 00:00 10/03/12 Filter Same As Above The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: ./ /' /f / /2b61 , I ~ ... d1i7f/~ [7 .. ~~ / ' Interim Branch Manager Digitally signed by Steve Carlston Date: 2012.11.13 17:30:07 -07:00 Page 1 of 22 www.energylab.com Analytical Ext:BHBflCB Sint:B 1952 CLIENT: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2012 Sample Delivery Group: C12100160 ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) ·DII· .... '·'t: .. U,· 1 • Billings, MT 800 .. 735-4489 • Casper, WY 888 .. 235 ... 0515 SI) 888-672-1225 • TX888-690-2218 Report Date: 11/10/12 CASE NARRATIVE Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by Ell reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-cs -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Tests associated with analyst identified as EU-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. Page 2of22 EN:RGY. L ABORATORIES www.energylab.com Ansf1tjcai ExceHence Since 1952 Helena, MT 877-412-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-686-7115 i Rapid City, SD 888-612-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: November 10,2012 PROJECT: 3rd Quarter Air 2012 SAMPLE ID: BHV-1 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C12040316-001 natu 7.87E-16 First Quarter 2012 230Th 2.64E-16 Air Volume in mLs 226Ra 3.95E-16 1.37E+ll 21Dpb 1.25E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C12070341-001 natu 1.86E-15 Second Quarter 2012 230Th 8.33E-16 Air Volume in mLs 226Ra 9.85E-16 1.33E+ll 21Dpb 9.55E-15 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C 12100 160-00 1 natu 1.06E-15 Third Quarter 2012 230Th 2.11E-16 Air Volume in mLs 226Ra 2.34E-16 1.36E+ll 21Dpb 1.13E-14 +LLD's are from Reg. Guide 4.14 Counting Precision JlCilmL N/A 3E-17 1E-17 1E-16 Counting Precision JlCilmL N/A 9E-17 5E-17 2E-16 Counting Precision pCilmL N/A 3E-17 2E-17 2E-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCJlCilmL N/A 6E-18 3E-18 4E-17 MDCJlCilmL N/A 7E-18 9E-18 6E-17 MDCJlCilmL N/A 8E-18 7E-18 4E-17 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration 1E-16 9E-14 8.75E-01 1E-16 3E-14 8.80E-01 1E-16 9E-13 4.39E-02 2E-15 6E-13 2.08E+00 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration 1E-16 9E-14 2.06E+00 1E-16 3E-14 2.78E+00 1E-16 9E-13 1.09E-01 2E-15 6E-13 1.59E+00 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration 1E-16 9E-14 1.18E+00 1E-16 3E-14 7.04E-01 1E-16 9E-13 2.60E-02 2E-15 6E-13 1.88E+00 Page 3 of 22 EI'.ER(iY. LABORATO RIES, WWN.energylab.com Analytical EXcel/snell SiiICS 1952 '~,'Mr81,1.~412707n .Sillings,MT 800 .. 735-4489 fI Casper, WY 888-235 .. 0515 ,,",', ,t!jj;d7$ ~ R~pip ~rty; 's[},888-672-1225 • College Station, lX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2012 Lab ID: C12100160-001 ClientSample ID BHV-1 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limtt. QCl -Quality controllimtt. Result 0.214 145 1540 21 5.B 31.9 2.7 0.9 29 3.9 1.1 MOC -Minimum detectable concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter Qualifiers Rl 0.0003 0.2 Report Date: 11/10/12 Collection Date: 10/01/12 DateReceived: 10/03/12 Matrix: Filter MCU QCl Method Analysis Date 1 By SW6020 10109/12 15:141 smm SW6020 10109/12 15:141 smm E909.0 10/30/12 14:201 eli-cs E909.0 10/30/12 14:201 eli-cs E909.0 10/30/12 14:20 1 eli-cs E903.0 10/17/12 12:371 Ibb E903.0 10/17/12 12:371 Ibb E903.0 10/17/12 12:371 Ibb E90B.0 10/17/1209:251 dmf E90B.0 10/17/1209:251 dmf E90B.0 10/17/1209:251 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 22 www.energylab.com Analytical ExceHence Since 1952 Helena, ,MT 877-412-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gi!lette, WY 86&-686-1115 • Rapid City, SO 888-612-1225 • College Station, TX 888-&90-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: November 10,2012 PROJECT: 3rd Quarter Air 2012 SAMPLE ID: BHV-2 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C 12040316-002 natu 4.22E-16 First Quarter 2012 230Th 1.15E-16 Air Volume in mLs 226Ra 2.77E-16 1.37E+11 21Dpb 1.58E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C12070341-002 natu 3.39E-16 Second Quarter 2012 230Th 1.56E-16 Air Volume in mLs 226Ra 1.74E-16 1.34E+ll 21Dpb 8.60E-15 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C12100160-002 Datu 3.13E-16 Third Quarter 2012 230Th 4.13E-17 Air Volume in mLs 226Ra 3.04E-17 1.36E+11 21Dpb 1.03E-14 +LLD's are from Reg. Guide 4.14 Counting Precision JlCilmL N/A 2E-17 9E-18 1E-16 Counting Precision JlCilmL N/A 2E-17 2E-17 2E-16 Counting Precision JlCilmL N/A 8E-18 7E-18 1E-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCJlCilmL N/A 4E-18 3E-18 4E-17 MDCJlCilmL N/A 5E-18 9E-18 6E-17 MDC JlCilmL N/A 4E-18 5E-18 4E-17 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration 1E-16 9E-14 4.68E-01 1E-16 3E-14 3.84E-01 1E-16 9E-13 3.07E-02 2E-15 6E-13 2.63E+00 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration 1E-16 9E-14 3.76E-01 1E-16 3E-14 5.19E-01 1E-16 9E-13 1.94E-02 2E-15 6E-13 1.43E+00 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration 1E-16 9E-14 3.48E-01 1E-16 3E-14 1.38E-01 1E-16 9E-13 3.37E-03 2E-15 6E-13 l.72E+OO Page 5 of 22 EN:RGY LABORATORIES www.energylab.com Arialyticlf ExCBIIBIICB SiRCB 1952 .·DII .... ·I:~t-U·, 1 -Billings, MT QOO-735-4489 . Gasper, WY888-235-0515 Clty,Sfl888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2012 Lab ID: C12100160-002 Client Sample ID BHV-2 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0631 42.7 1410 20 5.B 4.1 0.9 0.7 5.6 1.1 0.52 MDC -Minimum detectable concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter Qualifiers Rl 0.0003 0.2 Report Date: 11/10/12 Collection Date: 10/01/12 DateReceived: 10/03/12 Matrix: Filter MCL! QCl Method Analysis Date / By SW6020 10109/1215:17/ smm SW6020 10109/12 15:17 1 smm E909.0 10/30/12 15:29 1 eli-cs E909.0 10/30/12 15:291 eli-cs E909.0 10/30/12 15:291 eli-cs E903.0 10/17/12 12:371 Ibb E903.0 10/17/12 12:371 Ibb E903.0 10/17/12 12:37 /lbb E90B.0 10/17/1209:251 dmf E90B.0 10/17/12 09:251 dmf E90B.0 10/17/1209:251 dmf MCl -Maximum contaminant level. N D -Not detected at the reporting limit. Page 6 of 22 'EN:RGY· LABORATORIES www.energylab.com AnB/Jtical Excellence Since 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-68&:7115 • Rapid City, SO 888-&72-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: November 10, 2012 PROJECT: 3rd Quarter Air 2012 SAMPLEID: BHV-4 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C 12040316-003 natU 2.51E-15 First Quarter 2012 230Th 5.02E-16 Air Volume in mLs 226Ra 2.27E-16 1. 36E+ 11 210pb 1.03E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C 12070341-003 natU 2.62E-15 Second Quarter 2012 230Th 1.23E-15 Air Volume in mLs 226Ra 2.97E-16 1.35E+11 210pb 9.27E-15 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C12100160-003 natu 4.05E-15 Third Quarter 2012 230Th 8.33E-16 Air Volume in mLs 226Ra 5.43E-16 1. 36E+ 11 210pb 1.21E-14 +LLD's are from Reg. Guide 4.14 Counting Precision JlCilmL N/A 6E-17 8E-18 lE-16 Counting Precision JlCilmL N/A lE-16 3E-17 2E-16 Counting Precision JlCilmL N/A 8E-17 3E-17 2E-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCJlCilmL N/A 9E-18 3E-18 4E-17 MDC JlCilmL N/A 6E-18 9E-18 6E-17 MDCJlCilmL N/A 9E-18 6E-18 4E-17 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration lE-16 9E-14 2.79E+00 lE-16 3E-14 1. 67E+00 lE-16 9E-13 2.52E-02 2E-15 6E-13 l.72E+OO L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration lE-16 9E-14 2.91E+00 lE-16 3E-14 4.lOE+00 lE-16 9E-13 3.30E-02 2E-15 6E-13 1. 55E+00 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration lE-16 9E-14 4.50E+00 lE-16 3E-14 2.78E+00 lE-16 9E-13 6.03E-02 2E-15 6E-13 2.02E+00 Page 7 of 22 EN:,RGY LABORATORIES www.energyiab.com Jt<· Analytical ExcsJI8flCB Sines 1952 , ~iieM,.Ml]n·412"pln -Billings, MT800 .. 735 .. 4489 . Gasper, WY 888 .. 235 .. 0515 Jf!it~J"y!y~Q"~~686~1f75 • Rapip qfty, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2012 Lab 10 : C12100160-003 Client Sample 10 BHV-4 Analyses TRACE METALS Uranium Uranium, Activity RAOIONUCLIOES lead 210 lead 210 preCision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.B13 551 1650 22 5.B 73.B 3.B 0.9 113 11 1.2 MOC -Minimum detectable concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter Qualifiers RL 0.0003 0.2 Report Date: 11/10/12 Collection Date: 10/01/12 OateReceived: 10/03/12 Matrix: Filter MCL! QCL Method Analysis Date / By SW6020 10109/12 15:191 smm SW6020 10109/12 15:191 smm E909.0 10/30/12 16:39 1 eli-cs E909.0 10/30/12 16:391 eli-cs E909.0 10/30/12 16:39 1 eli-cs E903.0 10/17/12 12:37 llbb E903.0 10/17/12 12:371 Ibb E903.0 10/17/12 12:37 1 Ibb E90B.0 10/17/12 09:251 dmf E90B.0 10/17/12 09:25 1 dmf E90B.0 10/17/12 09:25 1 dmf MCl -Maximum contaminant level. . NO -Not detected at the reporting limit. Page B of 22 ENERGY L ABORATORIES www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 0 Casper, WY 888-235-0515 . Gillette, WI 86~-68~-7115 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: November 10,2012 PROJECT: 3rd Quarter Air 2012 SAMPLE ID: BHV-5 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C 12040316-004 natu 5.52E-15 First Quarter 2012 230Th 3.24E-15 Air Volume in mLs 226Ra 1.79E-15 1.36E+11 210pb 1.55E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C12070341-004 natu 5.87E-15 Second Quarter 2012 230Th 3.06E-15 Air Volume in mLs 226Ra 1.21E-15 1.22E+11 210Pb 1.11E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C 12100 160-004 natu 6.73E-15 Third Quarter 2012 230Th 2.59E-15 Air Volume in mLs 226Ra 2.43E-15 1.36E+11 210Pb 1.30E-14 +LLD's are from Reg. Guide 4.14 Counting Precision JlCilmL N/A 3E-16 2E-17 1E-16 Counting Precision JlCilmL N/A 3E-16 6E-17 2E-16 Counting Precision JlCilmL N/A 2E-16 5E-17 2E-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDC JlCilmL N/A 2E-17 3E-18 4E-17 MDCJlCilmL N/A 2E-17 1E-17 7E-17 MDCJlCilmL N/A 2E-17 5E-18 4E-17 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration 1E..:16 9E-14 6. 13E+OO 1E-16 3E-14 1.08E+01 1E-16 9E-13 1.99E-01 2E-15 6E-13 2.58E+00 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration 1E-16 9E-14 6.52E+00 1E-16 3E-14 1.02E+01 1E-16 9E-13 1. 35E-01 2E-15 6E-13 1.85E+00 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration 1E-16 9E-14 7.48E+00 1E-16 3E-14 8. 62E+00 1E-16 9E-13 2.70E-01 2E-15 6E-13 2. 16E+00 Page 9 of 22 www.energylab.com Analytical Exesllsnell Sines 1952 EN:RGY LABORATORIES '.. '¥~!~nal-MT :BH .. 412~0711 -Billings, MT 800 .. 735 .. 4489 • Casper, W'f 888-235-0515 • < ~WIf!~1l;(8',6·:686.7fl·5 . Rapid City, so 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2012 Lab ID: C12100160-004 Client Sample ID BHV-5 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES Lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 1.35 915 1760 23 5.8 330 7.2 0.7 352 33 3.0 MOC -Minimum detectal:jle concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter Qualifiers RL 0.0003 0.2 Report Date: 11/10/12 Collection Date: 10/01/12 DateReceived: 10/03/12 Matrix: Filter MCL! QCL Method Analysis Date 1 By SW6020 10109/12 15:20 1 smm SW6020 10109/12 15:20 1 smm E909.0 10/30/12 17:481 eli-cs E909.0 10/30/12 17:48 1 eli-cs E909.0 10/30/12 17:48 1 eli-cs E903.0 10/17/12 12:37 /lbb E903.0 10/17/12 12:37 /lbb E903.0 10/17/12 12:37 /lbb E908.0 10/17/12 09:25 1 dmf E908.0 10/17/12 09:25 1 dmf E908.0 10/17/12 09:25 1 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 22 EN:RGY LABORATORIES www.energylab.com AnalTfical Excellence Since 1952 Helena, MT 877-472-0711 " Billings, MT 800-735-4489 • Casper, WY 888-235-0515 . Gillette, WY 866-686-7115 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: November 10, 2012 PROJECT: 3rd Quarter Air 2012 SAMPLE ID: BHV-6 QuarterlDate Sampled Concentration Radionuclide Air Volume /lCilmL C 12040316-005 natu 4.41E-15 First Quarter 2012 230Th 1.82E-15 Air Volume in mLs 226Ra 4.00E-16 1.36E+11 210Pb 1.50E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume /lCilmL C12070341-005 natu 6.42E-15 Second Quarter 2012 230Th 2.25E-15 Air Volume in mLs 226Ra 5.11E-16 1.26E+11 210pb 9.54E-15 QuarterlDate Sampled Concentration Air Volume Radionuclide /lCilmL C12100160-005 natu 6.63E-15 Third Quarter 2012 230Th 1.31E-15 Air Volume in mLs 226Ra 1.22E-15 1. 24E+ 11 210Pb 1.34E-14 +LLD's are from Reg. Guide 4.14 Counting Precision /lCilmL N/A 2E-16 1E-17 1E-16 Counting Precision /lCilmL N/A 2E-16 4E-17 2E-16 Counting Precision /lCilmL N/A 1E-16 4E-17 2E-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDC /lCilmL N/A 2E-17 3E-18 4E-17 MDC /lCilmL N/A 1E-17 1E-17 7E-17 MDC/lCilmL N/A 2E-17 6E-18 5E-17 L.L.D.+ Effluent Cone. * % Effluent /lCilmL /lCilmL Concentration 1E-16 9E-14 4.90E+00 1E-16 3E-14 6.08E+00 1E-16 9E-13 4.45E-02 2E-15 6E-13 2.50E+00 L.L.D.+ Effluent Cone. * % Effluent /lCilmL /lCilmL Concentration 1E-16 9E-14 7. 13E+OO 1E-16 3E-14 7.50E+00 1E-16 9E-13 5.67E-02 2E-15 6E-13 1.59E+00 L.L.D.+ Effluent Cone. * % Effluent /lCilmL /lCilmL Concentration 1E-16 9E-14 7.36E+00 1E-16 3E-14 4.36E+00 1E-16 9E-13 1.35E-01 2E-15 6E-13 2.23E+00 Page 11 of 22 EN:RGY, LABORATORIES www.energylab.com Analytical best/SliCB Sints 1952 .. . ."He!en.~, .. ~'J7I .. 472~Onl • Billings, MT 800 .. 735-4489 • Casper, WY 888-235 .. 0515 ·Gilrm~,W(8&6~.$:B6:7f15 -Rapid City, SI} 888-672-1225 • College Station, lX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2012 Lab 10: C12100160-005 Client Sample 10 BHV-6 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLI DES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 1.21 . 819 1650 22 5.9 151 5.1 0.7 162 16 1.9 MOC -Minimum detectable concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter Qualifiers RL 0.0003 0.2 Report Date: 11/10/12 Collection Date: 10101/12 DateReceived: 10103/12 Matrix: Filter MCL! QCL Method Analysis Date / By SW6020 10/09/12 15:22/ smm SW6020 10109/12 15:22 / smm E909.0 10/30/12 18:57 / eli-cs E909.0 10/30/12 18:57 1 eli-cs E909.0 10/30/12 18:57 1 eli-cs E903.0 10/17/12 14:10/1bb E903.0 10/17/1214:10/lbb E903.0 10/17/12 14:10 /lbb E908.0 10/17/12 09:25 / dmf E908.0 10/17/12 09:25 1 dmf E908.0 10/17/12 09:25 1 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 12 of 22 www.energylab.com Ana/Tfical ExceHence Since 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Giilette, WY 866-686-7175 -Rapid City, SO 888-612-1225 -College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: November 10, 2012 PROJECT: 3rd Quarter Air 2012 SAMPLE ID: Blank QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C 12040316-006 natU l.37E-17 First Quarter 2012 230Th 5.82E-18 Air Volume in mLs 226Ra 7.24E-18 l.36E+ll 21Dpb -5.71E-18 Counting Precision JlCilmL N/A 2E-18 2E-18 2E-17 Note: This sample uses 136,000,000 L of aIr volume for comparIson purposes. QuarterlDate Sampled Concentration Counting Radionuclide Precision Air Volume JlCilmL JlCilmL C12070341-006 natu 2.08E-17 N/A Second Quarter 2012 230Th 7.76E-18 2E-18 Air Volume in mLs 226Ra 2.00E-18 5E-18 l.36E+ll 21Dpb l.82E-17 4E-17 Note: This sample uses 136,000,000 L of aIr volume for comparISon purposes. QuarterlDate Sampled Concentration Counting Radionuclide Precision Air Volume JlCilmL JlCilmL C 12100 160-006 natU l.81E-17 N/A Third Quarter 2012 230Th 6.30E-18 2E-18 Air Volume in mLs 226Ra l.05E-18 3E-18 1.36E+11 21Dpb l.62E-17 3E-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCJlCilmL N/A 2E-18 3E-18 4E-17 MDCJlCilmL N/A 2E-18 9E-18 7E-17 MDCJlCilmL N/A 2E-18 6E-18 4E-17 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration 1E-16 9E-14 1.52E-02 lE-16 3E-14 l.94E-02 lE-16 9E-13 8.04E-04 2E-15 6E-13 -9.52E-04 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration lE-16 9E-14 2.31E-02 lE-16 3E-14 2.59E-02 lE-16 9E-13 2.22E-04 2E-15 6E-13 3.04E-03 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration lE-16 9E-14 2.02E-02 lE-16 3E-14 2.10E-02 lE-16 9E-13 1.17E-04 2E-15 6E-13 2.71E-03 Page 13 of 22 www.energylab.com Analytical ExCBIlsncl ShIes 1952 EN:RGY LABORATORIES LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2012 LablD: C12100160-006 Client Sample ID Blank Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Defin itions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0036 2.5 2.2 3.6 5.9 0.1 0.5 O.B 0.B6 0.31 0.29 MOC -Minimum detectable concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter Report Date: 11/10/12 Collection Date: 10101/12 DateReceived: 10103/12 Matrix: Filter MCU Qualifiers Rl QCl Method Analysis Date / By 0.0003 SW6020 10109/12 15:291 smm 0.2 SW6020 10109/12 15:29 1 smm U E909.0 10/30/12 20:07 1 eli-cs E909.0 10/30/12 20:07 1 eli-cs E909.0 10/30/12 20:07 1 eli-cs U E903.0 10/17/12 14:10 /lbb E903.0 10/17/12 14:101 Ibb E903.0 10/17/1214:10/1bb E90B.0 10/17/12 09:25 1 dmf E90B.0 10/17/12 09:25 1 dmf E90B.0 10/17/12 09:251 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 14 of 22 iEN:RGY LABORATORIES ww......energylab.com Analytical ucslltNic, SifJCB 1952 :-3! ".'. ~~~n~I_MT:Bjl;;4t27071i . Billings, MT 800 .. 735 .. 4489 · Casper, WY 888-235-0515 , :~~~~-~Y:"":6'';68~':1f7_~ -Rapip City, so 888-672-1225 • College Station, 1X 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2012 Analyte Count Result Units Method: E903.0 Sample 10: C12100037-004AMS Radium 226 Sample 10: C12100037-004AMSO Radium 226 Sample 10: LCS-35265 Radium 226 Sample 10: MB-35265 Radium 226 Radium 226 precision (±) Radium 226 MDC Qualifiers: RL -Analyte reporting limit. 3 Sample Matrix Spike 9.41 E-07 pCi/Filter Sample Matrix Spike Duplicate 8.74E-07 pCi/Filter Laboratory Control Sample 17.4 pCi/Filter Method Blank -0.06 pCi/Filter 0.2 pCilFilter 0.3 pCilFilter MDC -Minimum detectable concentration Report Date: 11/10/12 Work Order: C12100160 RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: R 165941 Run: BERTHOLD 770-1_121011A 10/17/12 09:26 99 70 130 Run: BERTHOLD 770-1 121011A 10/17/12 09:26 - 100 70 130 7.4 22.3 Run: BERTHOLD 770-1 121011 A 10/17/12 12:37 90 70 130 Run: BERTHOLD 770-1 121011A 10/17/12 12:37 U NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 15 of 22 EN:RGY LASORAT O RIES WWN.energylab.com An,fytlcalExcsllBncs Sines 1952 . , " .. ¥~~~~:~t W'B71 .. 412~D71 i -Billings, MT 800 .. 735~4489 • Casper, WY 888 .. 235-0515 j.~l!:':WY]§.~:7-,j,,6":7.115. ° Rapip City, SD 88~-672-1225 8 College Station, IX 888 .. 690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2012 Analyte Count Result Units Method: . E908.0 Sample 10: C12100250-002AMS Thorium 230 Sample 10: C12100250-002AMSO Thorium 230 Sample 10: LCS-35306 Thorium 230 Sample 10: MB-35306 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration Sample Matrix Spike 51.1 pCi/Filter Sample Matrix Spike Duplicate 50.1 pCilFilter Laboratory Control Sample 17.7 pCi/Filter Method Blank 0.1 pCi/Filter 0.1 pCi/Filter 0.2 pCilFilter Report Date: 11/10/12 Work Order: C12100160 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: ALPHANAL YST _121015A 104 70 130 Run: ALPHANAL YST _121015A 103 70 130 2.2 Run: ALPHANAL YST _121015A 108 80 120 Run: ALPHANAL YST _121015A NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: 35306 10/17/12 09:25 10/17/1209:25 30.3 10/17/12 09:25 10/17/12 09:25 U Page 16 of 22 EI\ERGY L ABORATORIES www.energylab.com AIiBIyticaI ExcsnsiiciJ Sines 1952 • MTln7;·47~~ .. D7 1· .Billings~MT BOD .. 735 .. 448.9 • Casper, WY 888 .. 235 .. 0515 City;S'D 888-672-1225 • Collegestation, TX888-6~O-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2012 Analyte Count Result Units Method: E909.0 Sample 10: MB-17273 Lead 210 Lead 210 precision (±) Lead 210 MDC Sample 10: LCS-17273 Lead 210 Sample 10: C12100242-001AMS Lead 210 Sample 10: C12100242-001AMSO Lead 210 Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration Method Blank 0.09 pCi/Filter 3 pCi/Filter 6 pCi/Filter Laboratory Control Sample 596 pCi/Filter Sample Matrix Spike 2790 pCi/Filter Sample Matrix Spike Duplicate 2760 pCi/Filter Report Date: 11/10/12 Work Order: C12100160 RL %REC Low Limit High Limit Run: SUB-T47886 Run: SUB-T47886 94 70 130 Run: SUB-T47886 97 70 130 Run: SUB-T47886 96 70 130 NO -Not detected at the reporting limit. RPO RPOLimit Qual 1.2 Batch: T _17273 10/30/12 12:01 U 10/30/12 13:11 10/30/12 22:25 1 0/30/12 23 :35 13.6 U -Not detected at minimum detectable concentration Page 17 of 22 '", EN:RGY l..ABORAT ORIES www.energyJab.com Analytical ExullBncB Sines 1952 , .' '~el~n!l,'Mt'B71~472~Dl11 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 r6iU~~~;~~-i<~6~.;j86:1fl~ ~ Rapid City,SD 888-672-1225 • College Station, 1X 888-6QO-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Air 2012 Analyte Count Result Method: SW6020 Units Report Date: 11/10/12 Work Order: C12100160 RL %REC Low Limit High Limit RPO RPOLimit Qual Analytical Run: ICPMS2-C _1210098 Sample 10: ICV Uranium Initial Calibration Verification Standard 10/09/12 12:18 Method: SW6020 Sample 10: MB-35306 Uranium Sample 10: LCS2-35306 Uranium Sample 10: C12100160-001AOIL Uranium Sample 10: C12100250-002AMS Uranium Sample 10: C12100250-002AMSO Uranium Qual ifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration 0.0488 mg/L Method 81ank 8E-05 mg/filter Laboratory Control Sample 0.0830 mg/filter Serial Dilution 0.253 mg/filter Sample Matrix Spike 0.0482 mg/filter Sample Matrix Spike Duplicate 0.0499 mg/filter 0.00030 98 90 110 8atch: 35306 Run: ICPMS2-C_121 0098 10/09/12 15:09 6E-05 Run: ICPMS2-C_121 0098 10/09/12 15:11 0.00030 83 75 125 Run: ICPMS2-C_1210098 10/09/12 15:16 0.0014 17 20 Run: ICPMS2-C_121 0098 10/09/12 15:36 0.00030 96 75 125 Run: ICPMS2-C 1210098 10/09/12 15:37 - 0.00030 99 75 125 3.6 20 ND -Not detected at the reporting limit. Page 18 of 22 EI'ERGY LABO~ATORIES tI.l~'" www.energylab.com.· ~ Alialytical ExcsJIBilcs SincB 1952 ~,. rift.'s1!":472;,Dlll •• Biliings, MT800-735-4489 • Casper, WY 888-23~-0515 GilL~tt~~~~~18-6 .. ij1~ • R.qll.j~ t itv, SD888.;672·-1225 • College Siation, 1X 888-690-2218 Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Dorian Quis Reviewed by: BL2000\swaldrop Reviewed Date: 10/5/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Temp Blank received? ContainerlTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes D NAOC Yes D Yes D C12100160 Date Received: 10/3/2012 Received by: tjp No D No D No D No D No D No D No D No D No D No D No D No D No D Carrier NDA name: Not Present D Not Present D Not Present 0 Not Applicable 0 No VOA vials submitted 0 Not Applicable 0 Page 19 of 22 lJ Q) co CD N o 9. N N EN:RGY aa Chain of Custody and Analytical Request Record Page --1--of ---!--. -...... ~ . 'I.-• _ ... -----••• -~ ................ ,.. ... _ •• --_~ ..... " ........... W'., Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: £ V\e-rfj i p ve.L~ .3 r~ Q0"". +er ,At. ;;2.0 I ;'t State: U-t' Yes fid' No 0 Report Mail Address: p. 0 _ {?ex {?O'1 Contact Name: Phone/Fax: Email: Sampler: (Please Print) ~l~A.~ vTI g"15l ( t;./J..r"'~""'-Pc....\.,v\.eJ" '135 678 ~;2.~i 6;:,...,-,. ~ .;..,. PD--l A;'\.t:.r Invoice Address: Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: Sp..~c. 5(;...~1!! Special Report/Formats: $ &00&11 W®D® OO[§®@~~[ID .. Contact ELI prior to 5:(1S:N-'A-0 Ci> RUSH sample submittal ~o UJ.r::. ~ for charges and Cooler 10(s): ~cc;gOI4; C ~ R scheduling -See ~ ._> 0 >.oro D DW D EDD/EDT(Electronic Data) ~cn~»l$ W Instruction Page 03:= m 0') :c "'0 RAiznP o POlWNVWTP Format: U c:: Comments: ~«~I.Q ~ :::'I U o .... all c: « a °c D 8tate: 0 LEVEL IV ~ ~(rlSg'&:: r-m ~ c o Other: 0 NELAC ~~I~~ ~ l-t... On Ice: Y N (J « :::'I :::J (1)-= (j) s: + ~ l-S Z15..«I~o -W E Custody Seal lij >1 ~~ Ci ~ \1 w ro On Bottle Y N ~ CJ) "C en i , t: On Cooler Y N m ~ ..-J , -H Intact Y N 1 (/) SAMPLE IDENTIFICATION Collection Collection MATRIX ~ ~ . ..A Signature (Name, Location, Interval, etc.) Date Time 0... Match Y N 1 )3-'A 'J. 6l-lv~' )I. I-)I i~ 2 15ti IJ "1. '-f. t. i.. )( I~ 3 13\-\ v-4 f.. '/.. ~ X ~ nnn 4 ~14v-5 i ~ 'I X ~ 5 BI-J.V-6 X X j.. ~ ~\~IOf)\ loO ~ ~ 6 .B l£A..A.. \L. I l-i. i. ;. ~ 7 ~ 8 ~ 9 lffi} .~ 10 c::::!l Custody Relinquished by (print): DatelTime: t=: ?u&---Received by (print): DatefTime: Signature: bAr#-j,r... t'~~ tolll,:1.. ,·,300 Record Relinquished by (print): DatelTime: Signature: Received by (print): DatelTime: Signature: MUST be .A.. Signed KQCQlvea DY Laooramry: ~~/~;::a../ CfI~ ~ ( 0 A;hre: -Id g; Sample Disposal: Return to Client: Lab Disposal: In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab,com for additional information, downloadable fee schedule, forms, and links. EN:RGY LABORATORIES www.energylab.com Analytical Excsflsncs SifJt:s 1852 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 January 29, 2013 Energy Fuels Resources (USA) Inc 225 Union Blvd Ste 600 ANALYTICAL SUMMARY REPORT Lakewood, CO 80228-1826 Workorder No.: C13010107 Project Name: 4th Quarter Air 2012 Energy Laboratories, Inc. Casper WY received the following 6 samples for Energy Fuels Resources (USA) Inc on 1/4/2013 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C1301 01 07-001 BHV-1 12/31/1200:00 01/04/13 Filter Composite of two or more samples Metals, Total Digestion, Total Metals Lead 210 Radium 226 Thorium, Isotopic C1301 01 07-002 BHV-2 12/31/1200:00 01/04/13 Filter Same As Above C1301 01 07-003 BHV-4 12/31/1200:00 01/04/13 Filter Same As Above C1301 01 07-004 BHV-5 12/31/1200:00 01/04/13 Filter Same As Above C1301 01 07-005 BHV-6 12/31/1200:00 01/04/13 Filter Same As Above C1301 01 07-006 Blank 12/31/1200:00 01/04/13 Filter Same As Above The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: l /" i" / /J / /' / ~~/~ Digitally signed by Steve Carlston c;6i7tfb~ {~;7r1;C~~ Date: 2013.01.29 15:29:02 -07:00 ./ ' Interim Branch Manager Page 1 of 21 www.energylab.com Analytical ExesHINICB Sines 7952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 11 Casperi WY 888-235-0515 Gillette, WY 88& .. &86-7175 • Ra id City, SD 888-672-1225 • College Station, lX 888-690-2218 CLIENT: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2012 Sample Delivery Group: C1301 01 07 Report Date: 01/29/13 CASE NARRATIVE Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-cs -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 21 'I; N: RGY LABORATORIES www.energylab.com Analytical Excellence Since 19S2 Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: January 29, 2013 PROJECT: 4th Quarter Air 2012 SAMPLE ID: BHV-1 QuarterlDate Sampled Concentration Air Volume Radionucli<J.e ,..CilmL C12040316-001 natU 7.87E-16 First Quarter 2012 230Th 2.64E-16 Air Volume in mLs 226Ra 3.95E-16 1.37E+11 210Pb 1.25E-14 QuarterlDate Sampled Concentration Air Volume Radionuclide ,..CilmL C12070341-001 natU 1.86E-15 Second Quarter 2012 230Th 8.33E-16 Air Volume in mLs 226Ra 9.85E-16 1.33E+1l 210Pb 9.55E-15 QuarterlDate Sampled Concentration Radionuclide Air Volume ,..CilmL C12100160-001 natu 1.06E-15 Third Quarter 2012 230Th 2.llE-16 Air Volume in mLs 226Ra 2.34E-16 1.36E+11 210Pb 1.13E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume ,..CilmL C13010107-001 natU 6.86E-16 Fourth Quarter 2012 230Th 1.27E-16 Air Volume in mLs 226Ra 1.38E-16 1.37E+11 210Pb 1.54E-14 +LLD's are from Reg. Guide 4.14 Counting Precision ,..CilmL N/A 3E-17 1E-17 1E-16 Counting Precision ,..CilmL N/A 9E-17 5E-17 2E-16 Counting Precision ,..CilmL N/A 3E-17 2E-17 2E-16 Counting Precision ,..CilmL N/A 2E-17 1E-17 1E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDC,..CilmL N/A 6E-18 3E-18 4E-17 MDC,..CilmL N/A 7E-18 9E-18 6E-17 MDC,..CilmL N/A 8E-18 7E-18 4E-17 MDC,..CilmL N/A 9E-18 6E-18 5E-17 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 8.75E-01 1E-16 3E-14 8.80E-01 1E-16 9E-13 4.39E-02 2E-15 6E-13 2.08E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 2.06E+00 1E-16 3E-14 2.78E+00 1E-16 9E-13 1.09E-01 2E-15 6E-13 1.59E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 1.18E+00 1E-16 3E-14 7.04E-01 1E-16 9E-13 2.60E-02 2E-15 6E-13 1.88E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 7.62E-01 1E-16 3E-14 4.22E-01 1E-16 9E-13 1.53E-02 2E-15 6E-13 2.56E+00 Page 3 of 21 .'EI'l:~GV LABORATORIES www.energylab.com ~Helena.MT871 .. 472-0711 I1 Billings.MT 800 .. 735-4489 . Gasper, WY 888-235-0515 AnalyticalExCBlIsncBSiIlCB 195,2 J} . Gillette, WY 866-&86-7175 • Rapid City, so 888-612-1225 • College station, lX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2012 Lab 10: C1301 01 07-001 Client Sample 10 BHV-1 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.138 93.7 2100 19 6.7 18.9 2.0 0.8 17 3.0 1.2 MOC -Minimum detectable concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter Qualifiers Rl 0.0003 0.2 Report Date: 01/29/13 Collection Date: 12131/12 DateReceived: 01/04/13 Matrix: Filter MCL! QCl Method Analysis Date / By SW6020 01/18/13 04:58 1 elm SW6020 01/18/1304:581 clm E909.0 01/19/13 09: 13 1 eli-cs E909.0 01/19/1309:131 eli-cs E909.0 01/19/1309:131 eli-cs E903.0 01/21/1313:28/1bb E903.0 01/21/13 13:28 1 Ibb E903.0 01/21/1313:28/1bb E908.0 01/15/13 20:01 1 dmf E908.0 01/15/13 20:01 1 dmf E908.0 01/15/13 20:01 1 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 21 www.energylab.com Analytical ExceHence Since 1952 Helena, MT 877-472-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: January 29, 2013 PROJECT: 4th Quarter Air 2012 SAMPLE ID: BHV-2 Quarter/Date Sampled Concentration Radionuclide Air Volume ,..CilmL C 12040316-002 natu 4.22E-16 First Quarter 2012 230Th 1.15E-16 Air Volume in mLs 226Ra 2.77E-16 1.37E+ll 210Pb 1.58E-14 Quarter/Date Sampled Concentration RadiQnuciide Air Volume ,..CilmL C12070341-002 natU 3.39E-16 Second Quarter 2012 230Th 1.56E-16 Air Volume in mLs 226Ra 1.74E-16 1.34E+ll 210Pb 8.60E-15 Quarter/Date Sampled Concentration Radionuclide Air Volume ,..CilmL C 12100 160-002 natU 3.13E-16 Third Quarter 2012 230Th 4.13E-17 Air Volume in mLs 226Ra 3.04E-17 1.36E+11 210Pb 1.03E-14 Quarter/Date Sampled Concentration Radionuclide Air Volume ,..CilmL C 130 10 107 -002 natU 2.76E-16 Fourth Quarter 2012 230Th 5.41E-17 Air Volume in mLs 226Ra 7.05E-17 1. 37E+ 11 210Pb 1.48E-14 +LLD's are from Reg. Guide 4.14 Counting Precision ,..CilmL N/A 2E-17 9E-18 1E-16 Counting Precision ,..CilmL N/A 2E-17 2E-17 2E-16 Counting Precision ,..CilmL N/A 8E-18 7E-18 1E-16 Counting Precision ,..CilmL N/A 9E-18 9E-18 1E-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDC,..CilmL N/A 4E-18 3E-18 4E-17 MDC,..CilmL N/A 5E-18 9E-18 6E-17 MDC,..CilmL N/A 4E-18 5E-18 4E-17 MDC,..CilmL N/A 3E-18 5E-18 5E-17 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 4.68E-01 1E-16 3E-14 3.84E-01 1E-16 9E-13 3.07E-02 2E-15 6E-13 2.63E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 3.76E-01 1E-16 3E-14 5.19E-01 1E-16 9E-13 1.94E-02 2E-15 6E-13 1.43E+00 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 3.48E-01 1E-16 3E-14 1.38E-01 1E-16 9E-13 3.37E-03 2E-15 6E-13 1. 72E+OO L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 3.07E-01 1E-16 3E-14 1.80E-01 1E-16 9E-13 7.84E-03 2E-15 6E-13 2.47E+00 Page 5 of 21 EN:RGY LABORAT ORIES WWN.energylab.com Analytical Exesllencs Sines 1952 Helena, MT 871-472-0711 • Billings, MT 800-135-4489 • Casper, W'f 888-235-0515 Gillette, Wy 866-&86-7175 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2012 Lab ID: C1301 01 07-002 Client Sample ID BHV-2 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result I 0.0558 37.8 2020 18 6.7 9.6 1.3 0.7 7.4 1.3 0.46 MOC -Minimum detectable concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCilFilter pCi/Filter pCilFilter pCi/Filter pCi/Filter pCi/Filter pCi/Filter Qualifiers Rl 0.0003 0.2 Report Date: 01/29/13 Collection Date: 12/31/12 DateReceived: 01/04/13 Matrix: Filter MCL! QCl Method Analysis Date 1 By SW6020 01/18/1305:171 elm SW6020 01/18/1305:171 clm E909.0 01/19/1311 :181 eli-cs E909.0 01119/13 11 :181 eli-cs E909.0 01/19/1311 :181 eli-cs E903.0 01/21/1313:2811bb E903.0 01/21/1313:28/1bb E903.0 01/21/1313:28/1bb E908.0 01/15/1320:01 1 dmf E908.0 01/15/1320:01 1 dmf E908.0 01/15/1320:01 1 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 21 E~RGY L ABORATORIES www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: January 29, 2013 PROJECT: 4th Quarter Air 2012 SAMPLE ID: BHV-4 QuarterlDate Sampled Concentration Radionuclide Air Volume pCilmL C12040316-003 natu 2.51E-15 First Quarter 2012 230Th 5.02E-16 Air Volume in mLs 226Ra 2.27E-16 1.36E+ll 210Pb 1.03E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume pCilmL C12070341-003 natU 2.62E-15 Second Quarter 2012 230Th 1.23E-15 Air Volume in mLs 226Ra 2.97E-16 I 1.35E+ll 210Pb 9.27E-15 QuarterlDate Sampled Concentration Radionuclide Air Volume pCilmL C 12100 160-003 natU 4.05E-15 Third Quarter 2012 230Th 8.33E-16 Air Volume in mLs 226Ra 5.43E-16 1.36E+ll 210Pb 1.21E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume pCilmL C13010107-003 natu 2.32E-15 Fourth Quarter 2012 230Th 5.89E-16 Air Volume in mLs 226Ra 3.75E-16 1.35E+ll 210Pb 1.56E-14 +LLD's are from Reg. Guide 4.14 Counting Precision pCilmL N/A 6E-17 8E-18 lE-16 Counting Precision pCilmL N/A lE-16 3E-17 2E-16 Counting Precision pCilmL N/A 8E-17 3E-17 2E-16 Counting Precision pCilmL N/A 7E-17 2E-17 lE-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCpCilmL N/A 9E-18 3E-18 4E-17 MDC pCilmL N/A 6E-18 9E-18 6E-17 MDCpCilmL N/A 9E-18 6E-18 4E-17 MDC pCilmL N/A 2E-17 5E-18 5E-17 L.L.D.+ Effluent Conc. * % Effluent pCilmL pCilmL Concentration lE-16 9E-14 2.79E+00 lE-16 3E-14 1.67E+00 lE-16 9E-13 2.52E-02 2E-15 6E-13 l.72E+OO L.L.D.+ Effluent Conc. * % Effluent pCilmL pCilmL Concentration lE-16 9E-14 2.91E+00 lE-16 3E-14 4.lOE+00 lE-16 9E-13 3.30E-02 2E-15 6E-13 1.55E+00 L.L.D.+ Effluent Conc. * % Effluent pCilmL pCilmL Concentration lE-16 9E-14 4.50E+00 lE-16 3E-14 2.78E+00 lE-16 9E-13 6.03E-02 2E-15 6E-13 2.02E+00 L.L.D.+ Effluent Conc. * % Effluent pCilmL pCilmL Concentration lE-16 9E-14 2.58E+00 lE-16 3E-14 1.96E+00 lE-16 9E-13 4.16E-02 2E-15 6E-13 2.61E+00 Page 7 of 21 www.energylab.com ~Helena.MT877-472-0711 .Billings.MT 800-735-4489 . Gasper, WY 888-235-0515 AnalyticalfxcsllsnceSiIlClJ 1952 J' '" . Gillette, WY 866-&86-7175 • Rapid City, sa 888-&72-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2012 LablD: C1301 01 07-003 Client Sample ID BHV-4 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.462 313 2110 19 6.7 50.5 2.8 0.7 79 9.5 2.1 MOC -Minimum detectable concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter Qualifiers Rl 0.0003 0.2 Report Date: 01 /29/1 3 Collection Date: 12/31/12 DateReceived: 01/04/13 Matrix: Filter MCL! QCl Method Analysis Date 1 By SW6020 01/18/1305:201 clm SW6020 01/18/1305:201 clm E909.0 01/19/1313:231 eli-cs E909.0 01119/13 13:231 eli-cs E909.0 01/19/1313:231 eli-cs E903.0 01/21/13 13:281 Ibb E903.0 01/21/13 13:28 1 Ibb E903.0 01/21/1313:28/1bb E908.0 01/15/13 20:01 1 dll(lf E908.0 01/15/13 20:01 1 dmf E908.0 01/15/1320:01 1 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 8 of 21 www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-412-0111 ., Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-686-7115 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: January 29, 2013 PROJECT: 4th Quarter Air 2012 SAMPLE ID: BHV-5 Quarter/Date Sampled Concentration RadionucIide Air Volume p.1CilmL C 12040316-004 natu 5.52E-15 First Quarter 2012 230Th 3.24E-15 Air Volume in mLs 226Ra 1.79E-15 1.36E+11 210Pb 1.55E-14 Quarter/Date Sampled Concentration RadionucIide Air Volume p.1CilmL C12070341-004 natu 5.87E-15 Second Quarter 2012 230Th 3.06E-15 Air Volume in mLs 226Ra 1.21E-15 1.22E+11 210Pb 1.11E-14 Quarter/Date Sampled Concentration RadionucIide Air Volume p.1CilmL C 12100 160-004 natu 6.73E-15 Third Quarter 2012 230Th 2.59E-15 Air Volume in mLs 226Ra 2.43E-15 1.36E+11 210Pb 1.30E-14 Quarter/Date Sampled Concentration Radionuclide Air Volume p.1CilmL C 130 10 107 -004 natu 4.50E-15 Fourth Quarter 2012 . 230Th 1.62E-15 Air Volume in mLs 226Ra 1.79E-15 1.35E+11 210Pb 1.74E-14 +LLD's are from Reg. Guide 4.14 Counting Precision p.1CilmL N/A 3E-16 2E-17 1E-16 Counting Precision p.1CilmL N/A 3E-16 6E-17 2E-16 Counting Precision p.1CilmL N/A 2E-16 5E-17 2E-16 Counting Precision p.1CilmL N/A 2E-16 5E-17 1E-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCp.1CilmL N/A 2E-17 3E-18 4E-17 MDCp.1CilmL N/A 2E-17 1E-17 7E-17 MDCp.1CilmL N/A 2E-17 5E-18 4E-17 MDCp.1CilmL N/A 1E-17 5E-18 5E-17 L.L.D.+ Effluent Cone. * % Effluent p.1CilmL p.1CilmL Concentration 1E-16 9E-14 6. 13E+OO 1E-16 3E-14 1.08E+01 1E-16 9E-13 1.99E-01 2E-15 6E-13 2.58E+00 L.L.D.+ Effluent Cone. * % Effluent p.1CilmL p.1CilmL Concentration 1E-16 9E-14 6.52E+00 1E-16 3E-14 1.02E+01 1E-16 9E-13 1.35E-01 2E-15 6E-13 1.85E+00 L.L.D.+ Effluent Cone. * % Effluent p.1CilmL p.1CilmL Concentration 1E-16 9E-14 7.48E+00 1E-16 3E-14 8. 62E+00 1E-16 9E-13 2.70E-01 2E-15 6E-13 2. 16E+00 L.L.D.+ Effluent Cone. * % Effluent p.1CilmL p.1CilmL Concentration 1E-16 9E-14 5.00E+00 1E-16 3E-14 5.41E+00 1E-16 9E-13 1. 99E-01 2E-15 6E-13 2.91E+00 Page 9 of 21 EN:~GY LABORATORIES WWN.energylab.com r Analyticaf Exes/fsncB Sines 1952 ). Helena, MT 877-472-0711 • Billings, MT 800-735-4489 11 Casper, WY 888-235-0515 Gillette, WY 866-686-7175 11 Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2012 Lab ID: C1301 01 07-004 Client Sample ID BHV-5 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES Lead 210 Lead 210 precision (±) Lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 0.899 609 2360 20 6.7 243 6.1 0.7 219 21 1.8 MOC -Minimum detectable concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCilFilter Qualifiers Rl 0.0003 0.2 Report Date: 01/29/13 Collection Date: 12131/12 DateReceived: 01/04/13 Matrix: Filter MCL! QCl Method Analysis Date / By SW6020 01/18/1305:231 clm SW6020 01/18/13 05:23 1 clm E909.0 01/19/13 15:28 1 eli-cs E909.0 01/19/1315:281 eli-cs E909.0 01/19/1315:281 eli-cs E903.0 01/21/1313:28/1bb E903.0 01/21/1313:28/1bb E903.0 01/21/1313:28/1bb E908.0 01/15/13 20:01 1 dmf E908.0 01/15/13 20:01 1 dmf E908.0 01/15/1320:01 1 dmf MCL -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 21 www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-68&-7175 • Rapid City, SD 888-672-1225 0 College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: January 29, 2013 PROJECT: 4th Quarter Air 2012 SAMPLE ID: BHV-6 QuarterlDate Sampled Concentration Radionuclide Air Volume J1CilmL C 12040316-005 natU 4.41E-15 First Quarter 2012 230Th 1.82E-15 Air Volume in mLs 226Ra 4.00E-16 1.36E+11 2lOPb 1.50E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume J1CilmL C12070341-005 natu 6.42E-15 Second Quarter 2012 230Th 2.25E-15 Air Volume in mLs 226Ra 5.11E-16 1.26E+11 2lOPb 9.54E-15 QuarterlDate Sampled Concentration Radionuclide Air Volume J1CilmL C 12100 160-005 natu 6.63E-15 Third Quarter 2012 230Th 1.31E-15 Air Volume in mLs 226Ra 1.22E-15 1.24E+ll 2lOPb 1.34E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume J1CilmL C13010107-005 natu 3.83E-15 Fourth Quarter 2012 230Th 1.18E-I5 Air Volume in mLs 226Ra 9.30E-16 1.35E+l1 2lOPb 1.60E-14 +LLD's are from Reg. Guide 4.14 Counting Precision J1CilmL N/A 2E-16 1E-17 1E-16 Counting Precision p.1CilmL N/A 2E-16 4E-17 2E-16 Counting Precision J1CilmL N/A 1E-16 4E-17 2E-16 Counting Precision J1CilmL N/A lE-16 3E-17 1E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21 0 MDC J1CilmL N/A 2E-17 3E-18 4E-17 MDC J1CilmL N/A 1E-17 1E-17 7E-17 MDCJ1CilmL N/A 2E-17 6E-18 5E-17 MDC J1CilmL N/A 2E-17 5E-18 5E-17 L.L.D.+ Effluent Cone. * % Effluent J1CilmL J1CilmL Concentration 1E-16 9E-14 4.90E+00 1E-16 3E-14 6.08E+00 lE-16 9E-13 4.45E-02 2E-15 6E-13 2.50E+00 L.L.D.+ Effluent Cone. * % Effluent J1CilmL J1CilmL Concentration 1E-16 9E-14 7. 13E+OO 1E-16 3E-14 7.50E+00 1E-16 9E-13 5.67E-02 2E-15 6E-13 1.59E+00 L.L.D.+ Effluent Cone. * % Effluent J1CilmL J1CilmL Concentration 1E-16 9E-14 7.36E+00 1E-16 3E-14 4.36E+00 1E-16 9E-13 1.35E-01 2E-15 6E-13 2.23E+00 L.L.D.+ Effluent Cone. * % Effluent J1CilmL J1CilmL Concentration 1E-16 9E-14 4.26E+00 lE-16 3E-14 3.93E+00 lE-16 9E-13 1.03E-01 2E-15 6E-13 2.66E+00 Page 11 of 21 IEI\ERGY LABORATORIES www.energylab.com Analytical Excel/eneB Sines 7952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 -Casper, WY 888-235-0515 Gillette, WY 866-686-7175 .. Rapid City, SD 888-672-1225 • College Station, lX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2012 LablD: C1301 01 07-005 Client Sample ID BHV-6 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.765 518 2160 19 6.7 126 4.6 0.7 159 16 2.0 MOC -Minimum detectable concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter Qualifiers Rl 0.0003 0.2 Report Date: 01/29/13 Collection Date: 12131/12 DateReceived: 01/04/13 Matrix: Filter MCL! QCl Method Analysis Date / By SW6020 01/18/13 05:261 elm SW6020 01/18/1305:261 elm E909.0 01/19/13 17:331 eli-cs E909.0 01/19/13 17:33 1 eli-cs E909.0 01119/13 17:331 eli-cs E903.0 01/21/13 13:281 Ibb E903.0 01/21/1313:28/1bb E903.0 01/21/1313:28/1bb E908.0 01/15/13 20:01 1 dmf E908.0 01/15/1320:01 1 dmf E908.0 01/15/1320:01 1 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 12 of 21 www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-472-0711 It Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Energy Fuels Resources (USA) Inc REPORT DATE: January 29, 2013 PROJECT: 4th Quarter Air 2012 SAMPLE ID: Blank QuarterlDate Sampled Concentration Radionuclide Air Volume J1CilmL C 12040316-006 natU l.37E-17 First Quarter 2012 230Th 5.82E-18 Air Volume in mLs 226Ra 7.24E-18 1.36E+ll 210Pb -5.71E-18 Counting Precision J1CilmL N/A 2E-18 2E-18 2E-17 Note: This sample uses 136,000,000 L of air volume for comparIson purposes. QuarterlDate Sampled Concentration Counting Radionuclide Precision Air Volume J1CilmL J1CilmL C12070341-006 natu 2.08E-17 N/A Second Quarter 2012 230Th 7.76E-18 2E-18 Air Volume in mLs 226Ra 2.00E-18 5E-18 1.36E+ll 210Pb l.82E-17 4E-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. QuarterlDate Sampled Concentration Counting Radionuclide Precision Air Volume J1CilmL J1CilmL C 12100 160-006 natu l.81E-17 N/A Third Quarter 2012 230Th 6.30E-18 2E-18 Air Volume in mLs 226Ra l.05E-18 3E-18 l.36E+ll 210Pb l.62E-17 3E-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. QuarterlDate Sampled Concentration Counting Radionuclide Precision Air Volume J1CilmL J1CilmL C13010107-006 natU 1.26E-17 N/A Fourth Quarter 2012 230Th 3.46E-18 2E-18 Air Volume in mLs 226Ra 5.04E-18 4E-18 1.36E+ll 210Pb -l.50E-17 3E-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCJ1CilmL N/A 2E-18 3E-18 4E-17 MDCJ1CilmL N/A 2E-18 9E-18 7E-17 MDC J1CilmL N/A 2E-18 6E-18 4E-17 MDCJ1CilmL N/A 2E-18 5E-18 5E-17 L.L.D.+ Effluent Conc. * % Effluent J1CilmL J1CilmL Concentration 1E-16 9E-14 1.52E-02 1E-16 3E-14 1.94E-02 lE-16 9E-13 8.04E-04 2E-15 6E-13 -9.52E-04 L.L.D.+ Effluent Conc. * % Effluent J1CilmL J1CilmL Concentration lE-16 9E-14 2.31E-02 lE-16 3E-14 2.59E-02 lE-16 9E-13 2.22E-04 2E-15 6E-13 3.04E-03 L.L.D.+ Effluent Conc. * % Effluent J1CilmL J1CilmL Concentration lE-16 9E-14 2.02E-02 lE-16 3E-14 2.1OE-02 lE-16 9E-13 1.17E-04 2E-15 6E-13 2.71E-03 L.L.D.+ Effluent Conc. * % Effluent J1CilmL J1CilmL Concentration lE-16 9E-14 l.40E-02 lE-16 3E-14 1.15E-02 lE-16 9E-13 5.60E-04 2E-15 6E-13 -2.49E-03 Page 13 of 21 '.ENSRGY_' LABORATORIES www.energyiab.com J' Analytical Excel/sacs Since '952 Helena, MT 877 .. 472-0711 • Billings, MT 800-735-4489 . Casper, WY 888 .. 235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 \\I College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2012 Lab ID: C1301 01 07-006 Client Sample 10 Blank Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0025 1.7 -2 3.9 6.7 0.7 0.5 0.7 0.47 0.22 0.24 MOC -Minimum detectable concentration Units mg/filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter pCi/Filter U Qualifiers RL 0.0003 0.2 Report Date: 01/29/13 Collection Date: 12/31/12 DateReceived: 01/04/13 Matrix: Filter MCL! QCL Method AnalYSis Date 1 By SW6020 01/18/1305:291 elm SW6020 01/18/1305:291 clm E909.0 01119/13 19:381 eli-cs E909.0 01119/13 19:381 eli-cs E909.0 01119/13 19:381 eli-cs E903.0 01/21/1313:28/1bb E903.0 01121/13 13:28/1bb E903.0 01121/13 13:28/1bb E908.0 01/15/1320:011 dmf E908.0 01115/13 20:01 1 dmf E908.0 01115/13 20:01 1 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 14 of 21 'EI'l:RGY LABORATORIES 'IIVNI.energyla b.com Analytical Excellence Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-612-1225 " College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2012 Analyte Count Result Units Method: E903.0 Sample 10: LCS-36193 Radium 226 Sample 10: MB-36193 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: C13010112-008AMS Radium 226 'Sample 10: C13010112-008AMSO Radium 226 Qualifiers: RL -Analyte reporting limit. Laboratory Control Sample 12.1 pCilFilter 3 Method Blank 0.02 pCi/Filter 0.2 pCi/Filter 0.3 pCi/Filter Sample Matrix Spike 7.09E-06 pCi/Filter Sample Matrix Spike Duplicate 7.28E-06 pCi/Filter MDC -Minimum detectable concentration Report Date: 01/29/13 Work Order: C1301 01 07 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: BERTHOLD 770-2_130114A 103 80 120 Run: BERTHOLD 770-2_130114A Run: BERTHOLD 770-2_130114A 87 70 130 Run: BERTHOLD 770-2_130114A 92 70 130 2.6 ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: 36193 01/21/1313:28 01/21/1313:28 U 01/21/1315:30 01/21/13 15:30 25.8 Page 15 of 21 WVM.energylab.com Analytical ExCSOsncB Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-&86-7175 It Rapid City, SD 888-672-1225 .. College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2012 Analyte Count Result Units Method: E908.0 Sample 10: C13010112-006AMS Thorium 230 Sample 10: C13010112-006AMSO Thorium 230 Sample 10: LCS-36193 Thorium 230 Sample 10: MB-36193 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Qualifiers: RL -Analyte reporting limit. Sample Matrix Spike 6.06E-06 pCi/Filter Sample Matrix Spike Duplicate 6.05E-06 pCi/Filter Laboratory Control Sample 13.7 pCi/Filter 3 Method Blank 0.2 pCi/Filter 0.1 pCi/Filter 0.1 pCi/Filter MDC -Minimum detectable concentration Report Date: 01/29/13 Work Order: C1301 01 07 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: ALPHANAL YST _130110B 90 70 130 ) Run:ALPHANALYST_130110B 90 70 130 0.0 Run:ALPHANALYST_130110B 84 80 120 Run:ALPHANALYST_130110B ND -Not detected at the reporting limit. Batch: 36193 01/15/13 20:02 01/15/13 20:02 30.5 01/15/1320:02 01/15/1320:02 Page 16 of 21 EN:R~ LABORATORIES www;energylab.com J. Analytical ExcetlBfWB Since 7952 . Helena, MT 877 -472-0711 • Billings, MT 800-735-4489 -Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2012 Analyte Count Result Units Method: E909.0 Sample 10: MB-17838 Lead 210 Lead 210 precision (±) Lead 210 MDC Sample 10: LCS-17838 Lead 210 Sample 10: T13010038-001AMS Lead 210 Sample 10: T13010038-001AMSO Lead 210 Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration Method Blank -2 pCi/Filter 4 pCi/Filter 7 pCi/Filter Laboratory Control Sample 129 pCi/Filter Sample Matrix Spike 2.90E-05 pCi/Filter Sample Matrix Spike Duplicate 2.88E-05 pCi/Filter Report Date: 01/29/13 Work Order: C1301 01 07 RL O/OREC Low Limit High Limit Run: SUB-T49086 Run: SUB-T49086 98 70 130 Run: SUB-T49086 100 70 130 Run: SUB-T49086 98 70 130 ND -Not detected at the reporting limit. RPO RPOLimit Qual 0.6 Batch: T _17838 01/18/13 22:48 U 01/19/1300:53 01/19/1305:03 01/19/1307:08 14.1 U -Not detected at minimum detectable concentration Page 17 of 21 11i~.---· www.energylab.com , . Helena, MTB77-472-071 t -Billings, MT 800-135-4489 • Casper, WV 888-235-0515 r--:-- Analytical ExesUsnCB Sines 1952 ".' , Gillette, WY 166-686-7175 • Rapid CiIy, SD 888-672-1225 • College Station, lJ( 888-&90-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 4th Quarter Air 2012 Report Date: 01/29/13 Work Order: C1301 01 07 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW6020 Sample 10: ICV Uranium Sample 10: ICSA Uranium Sample 10: ICSAB Uranium Method: SW6020 Sample 10: MB-36193 Uranium Sample 10: LCS2-36193 Uranium Sample 10: C13010106-001AMS Uranium Sample 10: C13010106-001AMSO Uranium Sample 10: C13010107-001AOIL Uranium Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Initial Calibration Verification Standard 0.0490 mg/L 0.00030 Interference Check Sample A 1.34E-05 mg/L 0.00030 Interference Check Sample AB 3.20E-06 mg/L 0.00030 Method Blank 0.0003 mg/filter 9E-06 Laboratory Control Sample 0.0922 mg/filter 0.00030 Sample Matrix Spike 5.38E-09 mg/filter 0.00030 Sample Matrix Spike Duplicate 5.33E-09 mg/filter 0.00030 Serial Dilution 0.129 mg/filter 0.00030 Analytical Run: ICPMS2-C_130117A 01/17/13 16:23 98 90 110 Run: ICPMS2-C_130117A Run: ICPMS2-C_130117A 92 85 115 Run: ICPMS2-C _130117 A 106 75 125 Run: ICPMS2-C_130117A 104 75 125 Run: ICPMS2-C_130117A 7.2 01/17/1316:26 01/17/1316:30 Batch: 36193 01/18/13 04:36 01/18/1304:39 01/18/13 04:49 01/18/1304:51 20 01/18/1305:01 20 NO -Not detected at the reporting limit. Page 18 of 21 '~.N:RGY LABORATORIES www.energylab.com Analytical fxcs/lSilCB Sincs 1952 Helena, MT 817-472-0711 • Billings, MT 800-735-4489 0 Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Tracy Judge Reviewed by: BL2000\kmilier Reviewed Date: 1/7/2013 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Temp Blank received? Container/Temp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes D Yes D Yes D C13010107 Date Received: 1/4/2013 Received by: tj No D No D No D No D No D No D No D No D No D No D No D No D No D Carrier NDA name: Not Present D Not Present D Not Present 0 Not Applicable 0 No VOA vials submitted 0 Not Applicable 0 Page 19 of 21 i r EI\ERGY •'. ---".:- -~ Chain of Custody and Analytical Request Record .,.. -'\ Company Name: ~"d~~ "F~~ Report Mail Address: PO \\0)( 80 ,\ 13t\ QA\~~~ ~~ gL\5lt I nvoice Address: ~~ PLEASE PRINT (Provide as much information as possible.l Project Name, PWS, Permit, Etc. I Sample Origin "iTh Q\A.o.'C'"tu It; I" 20' 2 State: \A"" Contact Name: 6-"'(t,'" p~ 1,.,er Invoice Contact & Phone: Phone/Fax: "'l ~S 67r 2.2.21 ~,,~ Email: Purchase Order: Page_l_of~ EPA/State Compliance: Yes 51 No 0 Sampler: (Please Print) <"tJ4!!1' H.'l .. ~~ Quote/Bottle Order: Special Report/Formats: s: &11[l&[b W~O@ rn~®QD~rn!ID .1 Contact ELI prior to RUSH sample submittal Dow DpOTWNVWTP o State: o Other:---- o EDD/EDT(Electronic Data) Format: ___ _ D LEVEL IV o NELAC SAMPLE IDENTIFICATION (Name. Location, Interval, etc_) Collection I Collection Date ... i..sih._ Cl '-~O(l)~ ~[Q~OI (u --> 0 »-:9 m (/) (tI ~ C"'''CIJ U) ::> 03:= ~ 0) u ...... J5I.Q .S '15 ....... &...IDI~ Q) (l) c::'-E~I~Ci E ~>m I t--> ::l..22<I~::::: zc. Q)~ ~ >1 en MATRIX t3.t\\) .. , l()l'l_I~.·JI7.1 ~ '/J?. I 1 ~ -~ 2 t\"'\l ... 2. d .1\ 3 g*\l ... 'i ~ 4 8Ih)-5 y 5 B}\\J-" ~ ~ 6 ~\an~ 'OJ tl1~ -+ ''£hl/'~ I t~ .. A- 7 8 9 10 Cu tod --I RE}gquished by(pr~n'f ,_ S Y -1':. rAA'-' "I)~ 'Dat~:~ I/S/Ji: _ID3O 1~l; ~1~1"i1)( _~I ~I ~I 'f ~1~'1~1~~ '!I~l ~I ~ l:i 11 L~-' 1- '" I~I'LI~ Daterrime: Signature: '-' j::' R for charges and C ;, scheduling -See W Instruction Page :r: "0 C) c: Comments: ::l U « e ..... ro ~ c: l-:l I-·5 w "0 ... W en (f) "0 c: en -H CI) Received by (print): Daterrime: Received by (print): Datemme: (& Receipt Temp AliA °C On Ice- Custody Seal On Bottle On Cooler Intact Signature Match ~ I~ I{Q} nnn ~ I~ l!!£; ~ ~ I~ kOi Y N i~ 1~~l1()IOI61 I~ Signafure: Signature: Record R,elinquished by (print): V MUST be l signature: Signed Sample Disposal: ReturnJQ Client: Lab Disposal: -,Jail I In certain circumstances. samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to com...u:.t~ dlYSiS requested. This serves as notice of this possibility_ All sub-contract data will be clearly notated on your analytical report. t-'~'-' ~' Visit our web site at www_energylab.com for additional information, downloadable fee schedule, forms, and links. Period: October 1,2012 through Der,ember 31, 2012 (4th Quarter 2012) 8399817 8399808 8399605 8399096 8399093 8399084 8399080 1001% 100.2% 10 8399074 1; 4.2464 8399809 4.5033 -0.2440 8399804 4.2195 0.1434 27967.0 8399097 4.3131 0.3282 28132.6 8399092 4.2899 0.-1360 28299.4 8399085 43308 0.0658 284680 8399079 4.3100 0.1789 28639.4 8399073 4.2778 28833.2 83998'10 4.4423 8399503 4.3946 8399098 4.6340 51931.2 8:399091 4.4426 52096.0 8399086 4.4855 52266.6 8399078 4.5110 52437.6 10 8399072 4.5016 52631.7 4.4200 52772.8 Period: October 1, 2012 through December 31, 2012 (4th Quarter2012} 8HV..e on stream % 99.0% 4.3585 8399811 43648 4.4152 46623 Ki99090 4.3869 8399087 4.4533 4.4854 10 4.4352 ALL SHV on stream % 99.5% 8399813 08-0cl-12 15-0cl-12 4.2394 8399812 15 .. 0ct·i2 22·00t-12 4.2219 83f19801 22-0ct-12 2So0ct-12 4.2052 8399100 29-0cl-12 05-Nov-12 4.3093 8399089 OS-Nov-12 12-Nov-12 4.3133 B399088 12·Nov·12 '19-Nov-'12 4.3173 8399082 19..Nov~'12 26-Nov-12 4.3264 8399075 26-Nov-12 03-D9C·12 4.3050 10 8399070 03-Dsc-12 '11-0ao-12 4.2615 11·D",c-12 17·0ec-12 4.3435 BHV-1 Total Volume 4.83E+06 BHV-2 Total Volume. 4.83E+06 27797.4 27987.0 28132.6 28299.4 284680 28639.4 PageZ BHV.S Total Volume 4.77E+06 1145.0 0.0 166.2 332.4 498.8 667.5 838.6 10:l2.6 Page 21 of 21 ATTACHMENT D AIR PARTICULATE LOADING GRAPHS AND SUPPORTING DATA 0 0 0 !=> ...... 0 0 0 ...... 0 0 0 ...... 0 0 0 ...... 0 0 0 ...... 0 0 0 0 1/5/2009 3/5/2009 5/5/2009 7/5/2009 9/5/2009 11/5/2009 '\ + 1/5/2010 j l> -. ""'" OJ (n :::c 3/5/2010 r1" < OJ ~ r1" 5/5/2010 -. + 0 ::::J OJ 7/5/2010 "'tJ :::c OJ < ""'" N r+ 9/5/2010 -. + n c: 11/5/2010 OJ OJ r1" :::c < tD l. 1/5/2011 r- + 0 3/5/2011 OJ c.. OJ :::c ::::J < 5/5/2011 (1Q In ........ + 7/5/2011 3 (1Q OJ ............. :::c 9/5/2011 3 < ~ w ......... 11/5/2011 1/5/2012 3/5/2012 5/5/2012 7/5/2012 9/5/2012 11/5/2012 0 0 ~ ...... a a ...... a 0 ...... 0 0 ...... 0 0 0 0 0 0 0 1/5/2009 3/5/2009 5/5/2009 7/5/2009 9/5/2009 - 11/5/2009 1/5/2010 Ol 3/5/2010 -1 ~~ ::I: < I 5/5/2010 -1 ~ ~ -a OJ 7/5/2010 -1 ~ ~ .... -. n 9/5/2010 c: + OJ 11/5/2010 .... tD OJ :::r: r-~ 1/5/2011 0 ...... OJ a. ~ 3/5/2011 -I . ~ • :l OQ 5/5/2011 -1 ,.-z..... ........ 3 7/5/2011 -1 I ..--~i2E: • CJQ --.....-. 3 9/5/2011 i ~ w ........ 11/5/2011 1/5/2012 3/5/2012 5/5/2012 7/5/2012 9/5/2012 11/5/2012 0 0 ~ ...... a a ...... a 0 ...... 0 0 ...... 0 0 0 0 0 0 0 1/5/2009 3/5/2009 5/5/2009 7/5/2009 9/5/2009 11/5/2009 1/5/2010 a:J 3/5/2010 -I IY • ~ < I 5/5/2010 -I -----N • .,., cu 7/5/2010 -I ~ ~ .... -. n 9/5/2010 1 r: + cu 11/5/2010 .... (1) OJ :c r-< 0 N 1/5/2011 cu c.. 3/5/2011 1 I ~-----::l (JQ - 5/5/2011 i I ~ ....-.- 3 7/5/2011 -I -.".-• (JQ , 3 9/5/2011 1 ~::z: w ........ • 11/5/2011 1/5/2012 3/5/2012 5/5/2012 7/5/2012 9/5/2012 11/5/2012 0 (::) 0 0 I-" 1/5/2009 'I 3/5/2009 5/5/2009 7/5/2009 9/5/2009 11/5/2009 1/5/2010 3/5/2010 · 5/5/2010 7/5/2010 9/5/2010 + 11/5/2010 OJ I < J:,. 1/5/2011 3/5/2011 5/5/2011 7/5/2011 9/5/2011 11/5/2011 1/5/2012 3/5/2012 5/5/2012 7/5/2012 9/5/2012 11/5/2012 ._-- ~ o (::) o I-" o 0 (::) I-" 0 0 ~ I-" I-" (::) 0 0 0 0 0 0 Cl ::I: < I ~ "tJ OJ .., ,.... -. n c: OJ ,.... tD r-o OJ c.. :1 C7Q ........ 3 C7Q """-3 w .......... 0 0 !=> ..... a a ..... a 0 ..... 0 0 ..... 0 0 0 0 0 0 0 1/5/2009 3/5/2009 5/5/2009 7/5/2009 9/5/2009 11/5/2009 1/5/2010 O:J 3/5/2010 -I --.::~ ::J: < I 5/5/2010 -I ~ U1 "'tJ OJ 7/5/2010 -I ~ ""'" r+ -. n 9/5/2010 -~ c:: + OJ r+ 11/5/2010 tD OJ :J: r-< 0 Ln 1/5/2011 OJ c.. 3/5/2011 i I ~_· :s C7Q 5/5/2011 -I ~ .. ......... 3 7/5/2011 -I r ...... -.... C7Q " 3 9/5/2011 -I ec:Ji::::: _ ...... w ......... 11/5/2011 1/5/2012 3/5/2012 5/5/2012 7/5/2012 9/5/2012 11/5/2012 0 0 !=> ~ 0 0 ~ 0 0 ~ 0 0 ~ 0 0 0 0 0 0 0 1/5/2009 3/5/2009 5/5/2009 7/5/2009 9/5/2009 11/5/2009 1/5/2010 txJ 3/5/2010 , ~ :J: < I 5/5/2010 -1 ,~ 0'\ "'C OJ 7/5/2010 , ~~ ~ r+ -. n 9/5/2010 n~ c: + OJ ~ 11/5/2010 tD OJ I r-< 0 0-, 1/5/2011 OJ c.. 3/5/2011 i I ·~ :::l CJQ 5/5/2011 , ~ ........ 3 7/5/2011 , ~Mb ... CJQ )( " 3 915/2011 1 ~~ w ........ 11/5/2011 1/5/2012 3/5/2012 5/5/2012 7/5/2012 9/5/2012 11/5/2012 Period: July 2, 2012 through October 1, 2012 (3rd Quarter 2012) BHV-1 on stream % 99.9% Week Filter Start Stop Stop # Number Date Date Gross Tare Net Time 1 8401109 2-Jul-12 9-Jul-12 4.5176 4.2175 0.3001 39577.6 2 8399900 09-Jul-12 16-Jul-12 4.4865 4.3079 0.1786 39745.4 3 8399894 16-Jul-12 23-Jul-12 4.4905 4.2950 0.1955 39914.5 4 8399886 23-Jul-12 30-Jul-12 4.4193 4.2069 0.2124 40080.3 5 8399883 30-Jul-12 6-Aug-12 4.5496 4.2280 0.3216 40249.7 6 8399877 06-Aug-12 13-Aug-12 4.4300 4.2408 0.1892 40416.0 7 8399869 13-Aug-12 20-Aug-12 4.5256 4.2086 0.3170 40585.2 8 8399865 20-Aug-12 27-Aug-12 4.3646 4.2019 0.1627 40752.9 9 8399856 27-Aug-12 4-Sep-12 4.4343 4.2550 0.1793 40946.5 10 8399853 04-Sep-12 1O-Sep-12 4.3701 4.2301 0.1400 41088.0 11 8399848 1O-Sep-12 17-Sep-12 4.3710 4.2570 0.1140 41261.4 12 8399838 17-Sep-12 24-Sep-12 4.5155 4.2397 0.2758 41425.6 13 8399835 24-Sep-12 1-0ct-12 4.3490 4.2569 0.0921 41592.3 Totals 91 2184.0 4.447969 4.241946 0.2060 BHV-2 on stream % 99.9% Week Filter Start Stop Stop # Number Date Date G ross Tare Net Time 1 8401108 02-Jul-12 09-Jul-12 4.6247 4.1518 0.4729 49779.4 2 8401101 09-Jul-12 16-Jul-12 4.5903 4.3412 0.2491 49947.5 3 8399895 16-Jul-12 23-Jul-12 4.4379 4.2574 0.1805 50116.2 4 8399887 23-Jul-12 30-Jul-12 4.4727 4.2306 0.2421 50282.1 5 8399882 30-Jul-12 06-Aug-12 4.5388 4.1939 0.3449 50451.8 6 8399876 06-Aug-12 13-Aug-12 4.6048 4.2118 0.3930 50618.4 7 8399870 13-Aug-12 20-Aug-12 4.5878 4.2169 0.3709 50787.6 8 8399864 20-Aug-12 27-Aug-12 4.5027 4.2900 0.2127 50955.1 9 8399857 27-Aug-12 04-Sep-12 4.5331 4.2662 0.2669 51148.6 10 8399852 04-Sep-12 10-Sep-12 4.4242 4.1974 0.2268 51290.1 11 8399847 10-Sep-12 17-Sep-12 4.4450 4.2406 0.2044 51463.5 12 8399839 17-Sep-12 24-Sep-12 4.4990 4.2208 0.2782 51626.3 13 8399834 24-Sep-12 01-0ct-12 4.3070 4.2040 0.1030 51794.1 Totals 91 2184.0 4.505231 4.23251 0.2727 BHV-4 on stream % 99.6% Week Filter Start Stop Stop # Number Date Date Gross Tare Net Time 1 8401107 02-Jul-12 09-Jul-12 4.7603 4.2085 0.5518 25113.7 2 8401102 09-Jul-12 16-Jul-12 4.5694 4.3351 0.2343 25279.3 3 8399896 16-Jul-12 23-Jul-12 4.5426 4.2675 0.2751 25445.2 4 8399888 23-Jul-12 30-Jul-12 4.4734 4.2175 0.2559 25613.8 5 8399881 30-Jul-12 06-Aug-12 4.4364 4.2416 0.1948 25782.1 6 8399875 06-Aug-12 13-Aug-12 4.3355 4.1948 0.1407 25948.7 7 8399871 13-Aug-12 20-Aug-12 4.5634 4.2109 0.3525 26117.7 8 8399863 20-Aug-12 27-Aug-12 4.4030 4.2260 0.1770 26285.7 9 8399858 27-Aug-12 04-Sep-12 4.4416 4.2454 0.1962 26479.1 10 8399851 04-Sep-12 10-Sep-12 4.3913 4.2581 0.1332 26620.6 11 8399846 10-Sep-12 17-Sep-12 4.4174 4.2731 0.1443 26794.1 12 8399840 17-Sep-12 24-Sep-12 4.4140 4.2032 0.2108 26958.9 13 8399833 24-Sep-12 01-0ct-12 4.2478 4.1508 0.0970 27125.7 Totals 91 2184.0 4.461238 4.23327 0.2280 BHV -5 on stream % 99.7% Week Filter Start Stop Stop # Number Date Date Gross Tare Net Time 1 8401106 02-Jul-12 09-Jul-12 4.5598 4.3284 0.2314 48910.9 2 8401103 09-Jul-12 16-Jul-12 4.6005 4.3804 0.2201 49076.8 3 8399897 16-Jul-12 23-Jul-12 4.5106 4.2876 0.2230 49243.8 4 8399889 23-Jul-12 30-Jul-12 4.4391 4.2085 0.2306 49412.1 5 8399880 30-Jul-12 06-Aug-12 4.6619 4.2452 0.4167 49580.9 6 8399874 06-Aug-12 13-Aug-12 4.4555 4.2230 0.2325 49747.3 7 8399872 13-Aug-12 20-Aug-12 4.4860 4.1438 0.3422 49916.3 8 8399862 20-Aug-12 27-Aug-12 4.3549 4.1870 0.1679 50084.2 9 8399859 27-Aug-12 04-Sep-12 4.3479 4.2185 0.1294 50277.7 10 8399850 04-Sep-12 10-Sep-12 4.5830 4.2650 0.3180 50419.3 11 8399845 10-Sep-12 17-Sep-12 4.3833 4.2638 0.1195 50592.7 12 8399841 17-Sep-12 24-Sep-12 4.4637 4.2059 0.2578 50757.4 13 8399832 24-Sep-12 01-0ct-12 4.3915 4.2253 0.1662 50924.3 Totals 91 2184.0 4.479823 4.2448 0.2350 BHV-1 Start Time 39410.4 39577.6 39745.4 39914.5 40080.3 40249.7 40416.0 40585.2 40752.9 40946.5 41088.0 41261.4 41425.6 BHV-2 Start Time 49612.5 49779.4 49947.5 50116.2 50282.1 50451.8 50618.4 50787.6 50955.1 51148.6 51290.1 51463.5 51626.3 BHV-4 Start Time 24949.7 25113.7 25279.3 25445.2 25613.8 25782.1 25948.7 26117.7 26285.7 26479.1 26620.6 26794.1 26958.9 BHV-5 Start Time 48746.9 48910.9 49076.8 49243.8 49412.1 49580.9 49747.3 49916.3 50084.2 50277.7 50419.3 50592.7 50757.4 Total Time 10032.6 10068.0 10143.6 9949.8 10162.2 9976.8 10155.0 10062.6 11610.6 8492.4 10401.6 9852.6 10005.0 130912.8 Total T Ime 10011.6 10087.8 10122.0 9949.8 10186.8 9994.2 10152.0 10047.6 11609.4 8492.4 10401.6 9768.0 10068.0 130891.2 Total Time 9840.6 9934.8 9957.6 10116.6 10097.4 9995.4 10137.6 10078.2 11605.2 8494.2 10407.6 9886.8 10009.2 130561.2 Total Time 9842.4 9949.2 10021.8 10096.2 10133.4 9980.4 10138.2 10078.2 11608.8 8496.0 10401.6 9886.8 10009.2 130642.2 Page 1 Total Volume: 4.81 E+06 Total Loading, Per Cent Liters mg/m3 On Stream SCFM 10,369,343 0.0289 99.5% 36.5 10,548,479 0.0169 99.9% 37.0 10,627,686 0.0184 100.6% 37.0 10,424,638 0.0204 98.7% 37.0 10,647,174 0.0302 100.8% 37.0 10,452,926 0.0181 99.0% 37.0 10,610,875 0.0299 100.7% 36.9 10,514,327 0.0155 99.8% 36.9 12,131,819 0.0148 100.8% 36.9 8,801,494 0.0159 98.3% 36.6 10,721,275 0.0106 103.2% 36.4 10,155,402 0.0272 97.7% 36.4 10,312,486 0.0089 99.3% 36.4 136,317,924 0.0197 99.9% 36.8 Total Volume: 4.81 E+06 Total Loading, Per Cent Liters mg/m3 On Stream SCFM 10,347,639 0.0457 99.3% 36.5 10,569,223 0.0236 100.1% 37.0 10,605,056 0.0170 100.4% 37.0 10,424,638 0.0232 98.7% 37.0 10,672,948 0.0323 101.1% 37.0 10,471,157 0.0375 99.1% 37.0 10,607,740 0.0350 100.7% 36.9 10,498,653 0.0203 99.7% 36.9 12,130,565 0.0220 100.8% 36.9 8,801,494 0.0258 98.3% 36.6 10,721,275 0.0191 103.2% 36.4 10,068,202 0.0276 96.9% 36.4 10,377,422 0.0099 99.9% 36.4 136,296,012 0.0261 99.9% 36.8 Total Volume: 4.80E+06 Total Loading, Per Cent Liters mg/m3 On Stream SCFM 10,170,899 0.0543 97.6% 36.5 10,408,922 0.0225 98.6% 37.0 10,432,810 0.0264 98.8% 37.0 10,599,398 0.0241 100.4% 37.0 10,579,282 0.0184 100.2% 37.0 10,472,414 0.0134 99.2% 37.0 10,592,694 0.0333 100.6% 36.9 10,530,627 0.0168 100.0% 36.9 12,126,177 0.0162 100.7% 36.9 8,803,360 0.0151 98.3% 36.6 10,727,459 0.0135 103.2% 36.4 10,190,653 0.0207 98.1% 36.4 10,316,815 0.0094 99.3% 36.4 135,951,509 0.0219 99.6% 36.8 Total Volume: 4.80E+06 Total Loading, Per Cent Liters mQ/m3 On Stream SCFM 10,172,759 0.0227 97.6% 36.5 10,424,009 0.0211 98.7% 37.0 10,500,074 0.0212 99.4% 37.0 10,578,024 0.0218 100.2% 37.0 10,617,000 0.0392 100.5% 37.0 10,456,698 0.0222 99.0% 37.0 10,593,321 0.0323 100.6% 36.9 10,530,627 0.0159 100.0% 36.9 12,129,938 0.0107 100.8% 36.9 8,805,226 0.0361 98.3% 36.6 10,721,275 0.0111 103.2% 36.4 10,190,653 0.0253 98.1% 36.4 10,316,815 0.0161 99.3% 36.4 136,036,419 0.0228 99.7% 36.8 Period: July 2,2012 through October 1,2012 (3rd Quarter 2012) BHV-6 on stream % Week Filter Start # Number Date 1 8401105 02-Jul-12 2 8401104 09-Jul-12 3 8399898 16-Jul-12 4 8399890 23-Jul-12 5 8399879 30-Jul-12 6 8399873 06-Aug-12 7 8399867 13-Aug-12 8 8399861 20-Aug-12 9 8399860 27-Aug-12 10 8399849 04-Sep-12 11 8399844 10-Sep-12 12 8399842 17-Sep-12 13 8399831 24-Sep-12 Totals 91 ALL BHV on stream % Week # Blanks Start Date ~ 8399899 02-Jul-12 2 8399893 09-Jul-12 3 8399885 16-Jul-12 4 8399884 23-Jul-12 5 8399878 30-Jul-12 6 8399868 06-Aug-12 7 8399866 13-Aug-12 8 8399855 20-Aug-12 9 8399854 27-Aug-12 10 8399843 04-Sep-12 11 8399837 10-Sep-12 12 8399836 17-Sep-12 13 8399830 24-Sep-12 Totals 91 90.6% Stop D ate 09-Jul-12 16-Jul-12 23-Jul-12 30-Jul-12 06-Aug-12 13-Aug-12 20-Aug-12 27-Aug-12 04-Sep-12 10-Sep-12 17-Sep-12 24-Sep-12 01-0ct-12 2184.0 97.9% Stop Date 09-Jul-12 16-Jul-12 23-Jul-12 30-Jul-12 06-Aug-12 13-Aug-12 20-Aug-12 27-Aug-12 04-Sep-12 10-Sep-12 17-Sep-12 24-Sep-12 01-0ct-12 2184.0 G ross 4.4972 4.6531 4.4034 4.4407 4.5044 4.4050 4.5435 4.4237 4.4806 4.3402 4.3330 4.4662 4.3622 4.450246 Net . 4.3979 J ~:B91 4.2139 4.2491 4.2048 4.2076 4.2159 4.2449 4.2770 4.1677 4.2296 4.2106 4.2472 4.2365 T are 4.2061 4.3709 4.2734 4.2413 4.2076 4.2053 4.2398 4.2418 4.2483 4.2303 4.2060 4.2164 4.2038 4.23777 N et 0.2911 0.2822 0.1300 0.1994 0.2968 0.1997 0.3037 0.1819 0.2323 0.1099 0.1270 0.2498 0.1584 0.2125 Stop T Ime 2014.2 2179.5 2346.5 2515.4 2683.8 2850.0 3019.0 3186.9 3187.0 136.8 310.0 474.8 641.6 BHV-6 Start T Ime 1850.2 2014.2 2179.5 2346.5 2515.4 2683.8 2850.0 3019.0 3186.9 0.0 136.8 310.0 474.8 Total T Ime 9840.0 9919.8 10020.0 10134.6 10102.8 9971.4 10137.6 10079.4 0.6 8206.2 10389.6 9888.6 10007.4 118698 Total Volume: 4.36E+06 Total L' Iters 10,170,279 10,393,206 10,498,188 10,618,257 10,584,939 10,447,269 10,592,694 10,531,881 627 8,504,878 10,708,906 10,192,509 10,314,960 123,558,591 Loading, Per Cent / 3 0 S mQlm n tream 0.0286 97.6% 0.0272 98.4% 0.0124 99.4% 0.Q188 100.5% 0.0280 100.2% 0.0191 98.9% 0.0287 100.6% 0.0173 100.0% 370.5328 0.0% 0.0129 95.0% 0.0119 103.1% 0.0245 98.1% 0.0154 99.3% 28.5213 91.6% Page 2 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 Period: October 1, 2012 through December 31,2012 (4th Quarter 2012) BHV-1 on stream % Week Filter # N b um er 1 8399829 2 8399824 3 8399818 4 8399807 5 8399806 6 8399095 7 8399094 8 8399083 9 8399081 10 8399075 11 8399065 12 8399063 13 8399058 Totals Start D ate 1-0ct-12 08-0ct-12 15-0ct-12 22-0ct-12 29-0ct-12 05-Nov-12 12-Nov-12 19-Nov-12 26-Nov-12 03-Dec-12 11-Dec-12 17-Dec-12 24-Dec-12 91 BHV-2 on stream % Week Filter Start # Number Date 1 8399828 01-0ct-12 2 8399823 08-0ct-12 3 8399817 15-0ct-12 4 8399808 22-0ct-12 5 8399805 29-0ct-12 6 8399096 05-Nov-12 7 8399093 12-Nov-12 8 8399084 19-Nov-12 9 8399080 26-Nov-12 10 8399074 03-Dec-12 11 8399066 11-Dec-12 12 8399062 17-Dec-12 13 8399057 24-Dec-12 Totals 91 BHV -4 on stream % Week Filter # N b um er 1 8399827 2 8399822 3 8399816 4 8399809 5 8399804 6 8399097 7 8399092 8 8399085 9 8399079 10 8399073 11 8399067 12 8399061 13 8399056 Totals Start D ate 01-0ct-12 08-0ct-12 15-0ct-12 22-0ct-12 29-0ct-12 05-Nov-12 12-Nov-12 19-Nov-12 26-Nov-12 03-Dec-12 11-Dec-12 17-Dec-12 24-Dec-12 91 BHV-5 on stream % Week Filter # N b um er 1 8399826 2 8399821 3 8399815 4 8399810 5 8399803 6 8399098 7 8399091 8 8399086 9 8399078 10 8399072 11 8399068 12 8399060 13 8399055 Totals Start D ate 01-0ct-12 08-0ct-12 15-0ct-12 22-0ct-12 29-0ct-12 05-Nov-12 12-Nov-12 19-Nov-12 26-Nov-12 03-Dec-12 11-Dec-12 17-Dec-12 24-Dec-12 91 100.1% Stop D t ae 8-0ct-12 15-0ct-12 22-0ct-12 29-0ct-12 5-Nov-12 12-Nov-12 19-Nov-12 26-Nov-12 3-Dec-12 11-Dec-12 17-Dec-12 24-Dec-12 31-Dec-12 2184.0 100.2% Stop Date 08-0ct-12 15-0ct-12 22-0ct-12 29-0ct-12 05-Nov-12 12-Nov-12 19-Nov-12 26-Nov-12 03-Dec-12 11-Dec-12 17-Dec-12 24-Dec-12 31-Dec-12 2184.0 98.8% Stop D t ae 08-0ct-12 15-0ct-12 22-0ct-12 29-0ct-12 05-Nov-12 12-Nov-12 19-Nov-12 26-Nov-12 03-Dec-12 11-Dec-12 17-Dec-12 24-Dec-12 31-Dec-12 2184.0 99.2% Stop D ate 08-0ct-12 15-0ct-12 22-0ct-12 29-0ct-12 05-Nov-12 12-Nov-12 19-Nov-12 26-Nov-12 03-Dec-12 11-Dec-12 17-Dec-12 24-Dec-12 31-Dec-12 2184.0 G ross T are N et 4.3481 4.2048 0.1433 4.3236 4.1938 0.1298 4.3494 4.2081 0.1413 4.4734 4.2463 0.2271 4.3803 4.2474 0.1329 4.4683 4.3031 0.1652 4.4480 4.3154 0.1326 4.4462 4.3008 0.1454 4.4831 4.2912 0.1919 4.4506 4.3270 0.1236 4.4074 4.3156 0.0918 4.4035 4.3277 0.0758 4.4106 4.3463 0.0643 4.414808 4.279038 0.1358 Gross Tare Net 4.4674 4.1876 0.2798 4.3764 4.2272 0.1492 4.4137 4.2221 0.1916 4.4843 4.2347 0.2496 4.5460 4.2409 0.3051 4.8766 4.3332 0.5434 4.5138 4.3412 0.1726 4.6285 4.3064 0.3221 4.5580 4.2586 0.2994 4.5734 4.2934 0.2800 4.5492 4.3469 0.2023 4.4478 4.3499 0.0979 4.4165 4.3249 0.0916 4.527046 4.28208 0.2450 G ross T are N t e 4.3582 4.2001 0.1581 4.3491 4.2182 0.1309 4.3754 4.2464 0.1290 4.2593 4.5033 -0.2440 4.3629 4.2195 0.1434 4.6393 4.3131 0.3262 4.4259 4.2899 0.1360 4.3966 4.3308 0.0658 4.4889 4.3100 0.1789 4.4080 4.2778 0.1302 4.4019 4.3019 0.1000 4.4063 4.3552 0.0511 4.4375 4.3431 0.0944 4.408408 4.30072 0.1077 G ross T are N et 4.3890 4.2002 0.1888 4.2922 4.1688 0.1234 4.3678 4.2052 0.1626 4.4423 4.2451 0.1972 4.3946 4.2488 0.1458 4.6340 4.2989 0.3351 4.4426 4.3082 0.1344 4.4855 4.3204 0.1651 4.5110 4.3066 0.2044 4.5016 4.3219 0.1797 4.4200 4.3242 0.0958 4.3826 4.2982 0.0844 4.4337 4.3457 0.0880 4.438223 4.27632 0.1619 Stop T Ime 41758.1 41926.0 42096.4 42263.9 42433.5 42601.2 42768.7 42937.3 43107.7 43301.7 43444.0 43606.7 43779.4 Stop Time 51960.3 52128.2 52298.5 52466.1 52635.0 52803.2 52970.5 53139.4 53309.4 53503.5 53646.0 53808.7 53981.6 Stop T Ime 27291.9 27459.7 27629.1 27797.4 27967.0 28132.6 28299.4 28468.0 28639.4 28833.2 28967.8 29112.0 29284.5 Stop T Ime 51090.6 51258.4 51427.6 51596.0 .51765.3 51931.2 52098.0 52266.6 52437.6 52631.7 52772.8 52917.4 53090.0 BHV-1 Start T Ime 41592.3 41758.1 41926.0 42096.4 42263.9 42433.5 42601.2 42768.7 42937.3 43107.7 43301.7 43444.0 43606.7 BHV-2 Start Time 51794.1 51960.3 52128.2 52298.5 52466.1 52635.0 52803.2 52970.5 53139.4 53309.4 53503.5 53646.0 53808.7 BHV-4 Start T Ime 27125.7 27291.9 27459.7 27629.1 27797.4 27967.0 28132.6 28299.4 28468.0 28639.4 28833.2 28967.8 29112.0 BHV-5 Start T Ime 50924.3 51090.6 51258.4 51427.6 51596.0 51765.3 51931.2 52098.0 52266.6 52437.6 52631.7 52772.8 52917.4 Total T Ime 9946.8 10075.8 10223.4 10050.0 10173.0 10061.4 10051.2 10116.6 10227.0 11640.6 8532.6 9764.4 10363.2 131226 Total Time 9971.4 10075.2 10221.6 10051.2 10135.2 10095.0 10033.8 10135.8 10203.6 11642.4 8552.4 9762.0 10373.4 131253 Total T Ime 9973.8 10068.0 10159.8 10102.8 10175.4 9936.6 10005.6 10118.4 10284.0 11623.2 8080.8 8649.6 10351.2 129529.2 Total T Ime 9981.0 10065.6 10155.0 10102.8 10156.8 9954.0 10006.8 10120.8 10260.0 11641.8 8470.2 8671.8 10356.0 129942.6 Total Volume: 4.83E+06 Total L· Iters 10,280,664 10,556,651 10,711,295 10,529,620 10,658,490 10,541,564 10,502,415 10,570,751 10,686,107 12,064,278 8,794,834 10,064,492 10,681,695 136,642,853 Loading, Per Cent / mQ,m3 On Stream 0.0139 98.7% 0.0123 100.0% 0.0132 101.4% 0.0216 99.7% 0.0125 100.9% 0.0157 99.8% 0.0126 99.7% 0.0138 100.4% 0.0180 101.5% 0.0102 101.0% 0.0104 98.8% 0.0075 96.9% 0.0060 102.8% 0.0129 100.1% Total Volume: 4.83E+06 Total Loading, Per Cent Liters mg/m3 On Stream 10,306,089 0.0271 98.9% 10,556,022 0.0141 100.0% 10,709,409 0.0179 101.4% 10,530,877 0.0237 99.7% 10,618,886 0.0287 100.5% 10,576,767 0.0514 100.1% 10,484,234 0.0165 99.5% 10,590,813 0.0304 100.6% 10,661,656 0.0281 101.2% 12,066,144 0.0232 101.1% 8,815,243 0.0229 99.0% 10,062,018 0.0097 96.8% 10,692,208 0.0086 .. 102.9% 136,670,366 0.0233 100.1% Total Volume: 4.76E+06 Total L· Iters 10,308,570 10,548,479 10,644,660 10,584,939 10,661,004 10,410,808 10,454,768 10,572,632 10,745,666 12,046,245 8,329,149 8,915,430 10,669,326 134,891,675 Loading, Per Cent / 3 0 S mg,m n tream 0.0153 98.9% 0.0124 99.9% 0.0121 100.8% -0.0231 100.2% 0.0135 100.9% 0.0313 98.6% 0.0130 99.3% 0.0062 100.4% 0.0166 102.0% 0.0108 100.9% 0.0120 93.5% 0.0057 85.8% 0.0088 102.7% 0.0104 98.8% Total Volume: 4.78E+06 Total L· Iters 10,316,011 10,545,964 10,639,631 10,584,939 10,641,516 10,429,038 10,456,022 10,575,139 10,720,588 12,065,522 8,730,517 8,938,312 10,674,273 135,317,474 Loading, Per Cent / 0 mQlm3 n Stream 0.0183 99.0% 0.0117 99.9% 0.0153 100.7% 0.0186 100.2% 0.0137 100.8% 0.0321 98.8% 0.0129 99.3% 0.0156 100.4% 0.0191 101.8% 0.0149 101.1% 0.0110 98.0% 0.0094 86.0% 0.0082 102.7% 0.0154 99.1% Page 1 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 Period: October 1, 2012 through December 31,2012 (4th Quarter 2012) BHV-6 on stream % Week Filter Start # Number Oate 1 8399825 01-0ct-12 2 8399820 08-0ct-12 3 8399814 15-0ct-12 4 8399811 22-0ct-12 5 8399802 29-0ct-12 6 8399099 05-Nov-12 7 8399090 12-Nov-12 8 8399087 19-Nov-12 9 8399077 26-Nov-12 10 8399071 03-0ec-12 11 8399069 11-0ec-12 12 8399059 17-0ec-12 13 8399054 24-0ec-12 Totals 91 ALL BHV on stream % Week # Blanks Start Oate 1 8399819 01-0ct-12 2 8399813 08-0ct-12 3 8399812 15-0ct-12 4 8399801 22-0ct-12 5 8399100 29-0ct-12 6 8399089 05-Nov-12 7 8399088 12-Nov-12 8 8399082 19-Nov-12 9 8399075 26-Nov-12 10 8399070 03-0ec-12 11 8399064 11-0ec-12 12 8399053 17-0ec-12 13 8399052 24-0ec-12 Totals 91 99.0% Stop o ate 08-0ct-12 15-0ct-12 22-0ct-12 29-0ct-12 05-Nov-12 12-Nov-12 19-Nov-12 26-Nov-12 03-0ec-12 11-0ec-12 17-0ec-12 24-0ec-12 31-0ec-12 2184.0 99.5% Stop Oate 08-0ct-12 15-0ct-12 22-0ct-12 29-0ct-12 05-Nov-12 12-Nov-12 19-Nov-12 26-Nov-12 03-0ec-12 11-0ec-12 17-0ec-12 24-0ec-12 31-0ec-12 2184.0 G ross 4.4214 4.3658 4.3585 4.3648 4.4152 4.6623 4.3869 4.4533 4.4854 4.4352 4.4154 4.4246 4.4102 4.430692 Net 4.2295 4.2394 4.2219 4.2052 4.3093 4.3133 4.3173 4.3264 4.3050 4.2615 4.3435 4.3230 4.3441 4.2876 BHV-6 Stop Start Tare Net Time Time 4.2160 0.2054 807.8 641.6 4.2376 0.1282 975.6 807.8 4.1919 0.1666 1145.0 975.6 4.1855 0.1793 1313.3 1145.0 4.2539 0.1613 166.2 0.0 4.3214 0.3409 332.4 166.2 4.3129 0.0740 498.8 332.4 4.3015 0.1518 667.5 498.8 4.2846 0.2008 838.6 667.5 4.3050 0.1302 1032.6 838.6 4.3298 0.0856 1174.4 1032.6 4.3408 0.0838 1318.5 1174.4 4.3338 0.0764 1491.0 1318.5 4.27805 0.1526 Page 2 Total Volume: 4.77E+06 Total Total Loading, Per Cent Time Liters mQ/m3 On Stream SCFM 9975.0 10,309,810 0.0199 99.0% 36.5 10068.6 10,549,107 0.0122 99.9% 37.0 10161.6 10,646,545 0.0156 100.8% 37.0 10099".8 10,581,796 0.0169 100.2% 37.0 9974.4 10,450,412 0.0154 99.0% 37.0 9969.0 10,444,754 0.0326 98.9% 37.0 9985.8 10,434,079 0.0071 99.1% 36.9 10118.4 10,572,632 0.0144 100.4% 36.9 10270.2 10,731,246 0.0187 101.9% 36.9 11638.8 12,062,413 0.0108 101.0% 36.6 8505.6 8,767,005 0.0098 98.4% 36.4 8646.6 8,912,338 0.0094 85.8% 36.4 10353.6 10,671,800 0.0072 102.7% 36.4 129767.4 135,133,936 0.0146 99.0% 36.8 ATTACHMENT E ENVIRONMENTAL GAMMA GRAPHS AND·SUPPORTING DATA I White Mesa Mill Ambient Gamma Levels Over Time I 50.00 ~----------------------------------------------------------------------------------------------------------------------------------~ 45.00 I .... 40.00 I II ... 35.00 I II .... I I ... I I .. 30.00 I-CD t:::: 25.00 CO :::J 0--E Q) 0:: 20.00 E 15.00 10.00 I " • .. II 5.00 I _IV w.n.r ..... I I ...... n F\ ,w. n... I \ W _ I I I I :l I I lo II • I -.t II 41:::J , • I , "PI o.oo ~ 30~Sep~81 05~JlJ/~83 04-Apr~85 03~Feb~8? 11~Oct~88 16~JlJ/~90 10-Apr~9< 13~Jan~94 16~Oct~95 8vlJ/~97 13-Apr~99 <O~Feb~01 15~Oct~O< 9~JlJ/~04 10~A,pr~06 31~De~O? <~Oct~09 VvHrrl2 M12SA, M/J~L Background (BHV-3) subtracted from BHV-1, BHV-2, BHV-4, BHV-5, and BHV--6 [=;=SHV-1 ~BHV-2 -+-BHV-3 _BHV-4 _BHV-5 ...... BHV-6 I White Mesa Mill Ambient Gamma LevelsO~er Time BHV-1 I 50.00 ,-----------------------------------------------------------------------------------------------------------------~ 45.00 +1------------------------------------------------------------------------------------------------------------------~ 40.00 +1--------------------------------------------------------------------------------------------------------------------------~ 35.00 +1--------------------------------------------------------------------------------------------------------------------------~ 30.00 I-a> t:: CO 25.00 ::J 0--E a> 0:::: 20.00 E 15.00 10.00 I II 5.00 I • I , I I • I . , Ill' I \ I , '" 000 I ~¥' ... -~ .. . I I I I I I I I i', ... I ~ .11111111111 I ~II ..-r I .......... SII A Ii=AIIIIIF-, I I ,~, I I ,-, I I I I I I I I I I I I I I I I I I 30~S 03~O 07~O 09~O 30~O t 30~S 8~Oct ep~81 ct~83 ct~85 ct~87 c ~89 ep~91 ~93 16~O 10~AI 12~o 24~O 3~Oct ct~95 Ivoll~97 ct~99 ct~01 ~03 17~Oct~05 30~Oct~07 2~Oct~09 DIREC, RADIA /JON Background (BHV-3) Subtracted from BHV-1 ~BHV-1 I White Mesa Mill Ambient Gamma Levels Over Time BHV-21 50.00~------------------------------------------------------------------------------------------------------~ 45.00 +I----------------------------------------------------------------------------------------------------~ 40.00+1--------------------------------------------------------------------------------------------------~ 35.00+1--------------------------------------------------------------------------------------------------~ 30.00 s.... (1) t co :::l tT 25.00 -E (1) 0:: E 20.00 15.00+1--------------------------~---------------------------------------------------------------------4 10.00 1 • 5.00 I 1£ " 'I W • .. 1T' 0.00 .. AI,..¥.j~i .• ~ •.•. lli¥;:u_ Iill .. ~,..II~ .. ~.~~JAaPlll t /4¥.~~ .... _ .•. ~I 30~Sep~81 03~Oct~83 07~OCt~85 09~Oct~87 30~06t~89 30~Sep~91 8~OCt~93 16~Oct~95 10~NOl/~97 12~Oct~99 24~Oct~01 3~Oct~03 17~Oct~05 30~Oct~07 2~Oct~09 DIF?~C/1?4 I %~ Background (BHV-3) Subtracted from BHV-2 ___ BHV=-2-·· ------------------] J I White Mesa Mill Ambient Gamma Levels Over Time BHV-31 50.00 ~--------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------~ 45.00 I • 40.00 +-" • 35.00 I " • I I ... I'. -----I 30.00 ~ (J) t co ::J 0-25.00 -E (J) 0:: E 20.00 15.00 I II - 10.00 +1-----------------------------------------------------------------------------------------------------------------------------------------i 5.00 +I------------------------------------------------------------------------------~---------------------------------------------------------1 0.00 ~,~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 30-Sep_81 03-0Ct_83 07_0Ct_ 85 09-0Ct_87 30-0Ct_89 30-Sep_91 8-0Ct-93 Background (BHV-3) 3-0ct-03 DIRJ:cr RADIA /fON 30-0Ct_07 2-0Cf-09 24-0ct_01 17_0Cf_ 05 16-0Cf_95 10-NOl/_97 12-0Cf_99 .------------------------_._-------- ~BHV-3 I White Mesa Mill Ambient Gamma Levels Over-nmeBHV4] 50.00 ,---------------------------------------------------------------------------------------------------------------------------~ 45.00 +1----------------------------------------------------------------------------------------------------------------------------------~ 40.00 +1--------------------------------------------------------------------------------------------------------------------------------~ 35.00 +1--------------------------------------------------------------------------------------------------------------------------------------~ 30.00 '-Q) 1:: 25.00 CO ~ C" -E Q) c:::: 20.00 E 15.00 10.00 5.00 0.00 ~ ~ ---iii iii i i i i ~ i i i6 i ~ i ~ .... I •• ~ ~ .... i ~ -i • .,. _ i • t6 ~ i it i i " • i t6 -i . wY'Aw:i ~i i ......... i t6.i ~' 30-Sep_81 03-0Ct_83 O?-Oct_85 09_0ct_8? 30-0Ct_89 30-Sep_91 8-0 ct_93 16_0ct_95 10-Noll_9? 12-0ct_99 24-0ct_01 3-0ct-03 1?_Oct_05 30-0ct_O? 2-0ct-09 DIReCI RADIA lION Background (BHV-3) Subtracted from BHV-4 _e_BHV-4 I White Mesa Mill Ambient Gamma Levels Over Time BHV-si 50.00 45.00 +1----------------------------------------------------------------------------------------------------------------, 40.00 +1-------------------------------------------------------------------------------------------------------------i 35.00 I r 30.00 10-(J) t CO :::J C-25.00 -... E (J) 0::: E 20.00 15.00 +I----------------------------------------------------------------------------------------------------~ 10.00 I • 5.00 I I , ,. ... , ~,. 11:....,..... ,.III n. ".. -..... I I :i I I ...... It "''' I :1 \ I 0.00 •• ii ";!;'i ::'.i i ••• i i .i .i i .i i .i i .i i .i • .ri A i 30~Sep~81 03~Oct~83 O?~Oct~85 09~Oct~8? 30~Oct~89 30~Sep~91 8~Oct~93 16~Oct~95 10~NolI~9? 12~Oct~99 24~Oct~01 3~Oct~03 1?~Oct~05 30~Oct~O? 2~Oct~09 DIRI2CI RA. DIAl/ON Background (BHV-3) Subtracted from BHV-5 ~BHV-5 I White Mesa Mill Ambient Gamma Levels Over Time BHV-sl 50.00 45.00 40.00 35.00 30.00 s..... Q) t CO 25.00 ::J 0--E Q) 0:: 20.00 E 15.00 I 10.00 5.00 0.00 ~ ~ ------- 30-Sep_81 03-0ct_83 07-0Ct_85 09-0ct_8? 30-0Ct_89 30-Sep_91 8-0ct-93 16-0ct_95 10-Noll_97 12-0ct_99 · 24-0ct_01 3-0ct-03 1?_Oct_05 30-0ct_O? 2-0ct-09 D/~ecr RADIA /JON Background (BHV-3) Subtracted from BHV-6 ___ BHV-6 White Mesa Mill Third Quarter 2012 Environmental Spherical Gamma Monitor Results Badge Number Location Control Administration Vault 1 V205 Control Room 2 BHV-6 3 Ore Stor. -Molycorp Area 4 Vanadium Precip.Area 5 Yellocake Drying Area 6 Leach 7 SAG Mill Control Room 8 Yellowcake Precip. 9 Central Control Room 10 Trommel Screen (ore pad) 11 North East Corner Ore Pad 12 Met. Lab 13 Filter Press Room 14 BHV-l 15 BHV-2 16 BHV-3 17 BHV-4 18 BHV-5 19 SAG Mill 20 Tails 21 CCD 22 North SX 23 Administration Building 24 Admin Parking Lot 25 26 27 28 29 30 31 32 33 34 45 46 47 51 52 53 64 Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scalehouse Sample Plant (OBS) Front Gate AF -Barrel Dump Station AF Circuit -South AF Circuit -North North Control # 1 North Control # 2 CaF2 Barrel Dump Station -Operator Station KF Barrel Dump Station Date Issued 6/26/2012 6/26/2012 612612012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 612612012 6126/2012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 612612012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 612612012 6126/2012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 612612012 6/26/2012 6/26/2012 6/26/2012 6/26/2012 612612012 6/26/2012 6/26/2012 Total Days Badge at Date Returned WMM 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 92 9/26/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 912612012 9/26/2012 9/26/2012 9/26/2012 912612012 9/~6/2012 92 92 92 92 92 92 92 92 92 92 92 92 92 92 92 92 92 Mean Ambient Dose Equivalent mRem 1 hour mRem 1 Day 33.5 0.02 0.364 55 0.02 0.598 32 0.01 0.348 198.4 97.8 275.4 361.1 153.8 78.2 156.7 271.2 70.8 211.9 32.6 31.3 30.9 31.4 34.5 413.4 65.5 80.2 83.6 36.9 100.3 1571.5 434.1 140.9 58 121.7 50.1 389.9 258.5 282.1 221.7 433.4 135.2 463.2 39.4 35.1 287.8 0.09 0.04 0.12 0.00 0.16 0.07 0.04 0.07 0.12 0.03 0.10 0.01 0.01 0.01 0.01 0.02 0.19 0.03 0.04 0.04 0.02 0.05 0.71 0.20 0.06 0.03 0.06 0.02 0.18 0.12 0.13 0.10 0.20 0.06 0.21 0.02 0.02 0.13 0.00 2.157 1.063 2.993 0.000 3.925 1.672 0.850 1.703 2.948 0.770 2.303 0.354 0.340 0.336 0.341 0.375 4.493 0.712 0.872 0.909 0.401 1.090 17.082 4.718 1.532 0.630 1.323 0.545 4.238 2.810 3.066 2.410 4.711 1.470 5.035 0.428 0.382 3.128 0.000 mReml Week 2.55 4.18 2.43 15.10 7.44 20.95 0.00 27.48 11.70 5.95 11.92 20.63 5.39 16.12 2.48 2.38 2.35 2.39 2.63 31.45 4.98 6.10 6.36 2.81 7.63 119.57 33.03 10.72 4.41 9.26 3.81 29.67 19.67 21.46 16.87 32.98 10.29 35.24 3.00 2.67 21.90 0.00 Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 51 52 53 64 White Mesa Mill Fourth Quarter 2012 Environmental Spherical Gamma Monitor Results Location Administration Vault V205 Control Room BHV-6 Ore Stor. -Molycorp Area Vanadium Precip.Area Yellocake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room Trommel Screen (ore pad) North East Comer Ore Pad Met. Lab Filter Press Room BHV-l BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scalehouse Sample Plant (OBS) Front Gate AF -Barrel Dump Station AF Circuit -South AF Circuit -North North Control # I North Control # 2 CaF2 Barrel Dump Station - Operator Station KF Barrel Dump Station Date Issued 9/26/2012 912612012 9126/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 912612012 9126/2012 9/26/2012 9/26/2012 9/26/2012 912612012 9/26/2012 912612012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 912612012 9126/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 912612012 9126/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 912612012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 9/26/2012 Date Returned 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 12/3112012 Mean Total Days Ambient Badge at Dose WMM Equivalent 96 33.1 96 60.3 96 30.2 96 174.1 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 96 90.7 240.8 184.8 297.9 152.4 93.3 272.7 60.9 196.3 34.8, 32.1 29.5 33.3 33.4 259.9 80.2 64.4 37.3 91 1279 385.3 121.6 59.6 99.4 48 401.6 224.1 274.4 207.9 146.6 50.6 108.8 37.3 32.4 155.3 mReml mReml hour Day 0.01 0.345 0.03 0.628 0.01 0.315 0.08 1.814 0.04 0.10 0.08 0.13 0.07 0.04 0.00 0.12 0.03 0.09 0.02 0.01 0.01 0.01 0.01 0.11 0.00 0.03 0.03 0.02 0.04 0.56 0.17 0.05 0.03 0.04 0.02 0.17 0.10 0.12 0.09 0.06 0.02 0.05 0.02 0.01 0.00 0.07 0.945 2.508 1.925 3.103 1.588 0.972 0.000 2.841 0.634 2.045 0.363 0.334 0.307 0.347 0.348 2.707 0.000 0.835 0.671 0.389 0.948 13.323 4.014 1.267 0.621 1.035 0.500 4.183 2.334 2.858 2.166 1.527 0.527 1.133 0.389 0.338 0.000 1.618 mReml Week 2.41 4.40 2.20 12.69 6.61 17.56 13.48 21.72 11.11 6.80 0.00 19.88 4.44 14.31 2.54 2.34 2.15 2.43 2.44 18.95 0.00 5.85 4.70 2.72 6.64 93.26 28.09 8.87 4.35 7.25 3.50 29.28 16.34 20.01 15.16 10.69 3.69 7.93 2.72 2.36 0.00 11.32 ATTACHMENT F VEGETATION GRAPHS, DATA TABLE, LABORATORY RESULTS AND QAlQC (Log Scale) ~ 6 6 6 6 6 6 0 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 0:> ---J (j) (J'1 ~ eN N 8/27/1981 8/27/1982 8/27/1983 8/27/1984 8/27/1985 8/27/1986 8/27/1987 8/27/1988 , :::0 8/27/1989 --I I ~ S» I N N 8/27/1990 -i ~ en 0 8/27/1991 --I ~ 0 ::l 8/27/1992 --I ~ C') CD ::l .... 8/27/1993 --I ~I .. S» ~ 8/27/1994 0 t ::l en 8/27/1995 z ::l m < 8/27/1996 CD (Q T 8/27/1997 CD .... S» z 8/27/1998 ~ ~ 0 ::l 8/27/1999 -t c 8/27/2000 0 :::: (f) " ~ 8/27/2001 (Q - 8/27/2002 8/27/2003 8/27/2004 8/27/2005 8/27/2006 8/27/2007 8/27/2008 8/27/2009 8/27/2010 8/27/2011 8/27/2012 (Log Scale) 6 6 6 6 6 6 6 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 (X) ---.J 0> (]I ~ W N 8/27/1981 8/27/1982 8/27/1983 8/27/1984 8/27/1985 8/27/1986 8/27/1987 8/27/1988 . "'tJ 8/27/19891 ~~ C'" I ~ ..;/I, 8/27/1990 j I...J{I " 0 0 8/27/1991 0 :::l 8/27/19921 ~ () (1) :::l ..... 8/27/19931 • ~~. I ., S» ..... 8/27/1994 O· t :::l til 8/27/1995 z :::l m < 8/27/1996 (1) T CQ 8/27/1997 (1) ..... S» z 8/27/1998 ..... :z: O· :::l 8/27/1999 -f c: 8/27/2000 0 :::::..: (J) " :z: 8/27/2001 CQ - 8/27/2002 8/27/2003 8/27/2004 8/27/2005 8/27/2006 8/27/2007 8/27/2008 8/27/2009 8/27/2010 8/27/2011 8/27/2012 (Log Scale) -....... 6 6 6 6 6 6 6 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 00 ....... 0> 01 ~ VJ N 01-Jan-81 01-Jan-82 j I M :e ::I: 01-Jan-83 • =i m 01-Jan-84 s: 01-Jan-85 --I ~ ___....____1 m en 01-Jan-86 --I I~---r--.. :t> s: 01-Jan-87 ~ I ~ r-r- 01-Jan-88 Z 01-Jan-89 --I ~ 0 :::c 01-Jan-90 --I ~ -I ::I: m 01-Jan-91 --I 1/ Z :t> en 01-Jan-92 --I I _=_==='----,. -I 0 t 01-Jan-93 ." s: ;;0 01-Jan-94 r-Q) -r-r0 01-Jan-95 ~:::c N (j) _.1» 01-Jan-96 -I T ,,~ (Q~ 01-Jan-97 -en "'U I» 0-::l ~ 01-Jan-98 Q. 0 01-Jan-99 "'C C'" I 01-Jan-OO ~ ....a. 0 01-Jan-01 (1 0 01-Jan-02 --I ~~ ::l (") CD 01-Jan-03 --I ..J. .=r-::l .... .... 01-Jan-04 --I I ----......~ I» .... o· 01-Jan-05 ::l (J) 01-Jan-06 ::l 01-Jan-07 < CD (Q 01-Jan-08 CD .... I» .... 01-Jan-09 1 .. ~:=T:=::'"'' o· ::l 01-Jan-10 01-Jan-11 01-Jan-12 6 6 6 0 0 0 m m m I I I 0 0 0 ex> "-I 0> 01-Jan-81 01-Jan-82 01-Jan-83 01-Jan-84 01-Jan-85 01-Jan-86 01-Jan-87 01-Jan-88 01-Jan-89 01-Jan-90 01-Jan-91 01-Jan-92 fl 01-Jan-93 ;;u 01-Jan-94 Q) N N 01-Jan-95 0> T 01-Jan-96 "'tl 01-Jan-97 0" ~ 01-Jan-98 01-Jan-99 01-Jan-OO 01-Jan-01 01-Jan-02 01-Jan-03 01-Jan-04 01-Jan-05 01-Jan-06 01-Jan-07 01-Jan-08 01-Jan-09 01-Jan-10 01-Jan-11 01-Jan-12 (Log Scale) 6 6 0 0 m m I I 0 0 O'l ,t:.. o o m I o (,.) o o m I o I\.) ,-~~ :e ::I: =i m s: m en » s: r-r- z o ~ ::I: :e m en -I o "T1 s: r--r-~;tJ _.Q) -. "I\) (QI\) -en Q) :::l C. ""D C'" • I\) ~ o o o :::l (") (I) :::l ,.... CJ !:r. o :::l tn :::l < (I) (Q (I) Dr ,.... o· :::l (Log Scale) 6 6 6 6 6 6 6 6 6 0 0 0 0 0 0 0 0 0 m m m m m m m m m I I I I I I I I + 0 0 0 0 0 0 0 0 0 ex> '" 0) O'l ~ W N ~ 0 01-Jan-81 I I :e 01-Jan-82 i I ~ I ~ J: =i 01-Jan-83 m s: 01-Jan-84 m en 01-Jan-85 » 01-Jan-86 s: • 01 -Jan-S71 (~ • 01-Jan-88 en 0 C 01-Jan-89 -I J: 01-Jan-90 i ~ 1 ~ :e m 01-Jan-91 en -I 01-Jan-92 0 t ." 01-Jan-93 s: :::0 01-Jan-94 • Q) C". N I\) 01-Jan-95 OAJ 0'> -'1» -. T 01-Jan-96 "I\) (QI\) -0') ""0 01-Jan-97 I» 0" N ::l --" 01-Jan-98 c. 0 "'tJ 01-Jan-99 C" • I\) 01-Jan-OO i I ~ ~ 0 01-Jan-01 i _I~ [II 0 0 01-Jan-02 i ~ ~ ::l (') (I) 01-Jan-03 i _. »1 7'=11 ::l ~ ""'I I» 01-Jan-04 i _I 1'2' ~ 0 01-Jan-05 i I ~ ::l en 01-Jan-06 ::l < 01-Jan-07 (I) (Q 01-Jan-08 (I) ~ I» ~ 01-Jan-09 o· ::l 01-Jan-10 01-Jan-11 01 -Jan-12 WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHEAST OF MILL SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd '82 lS-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nov-82 2nd '83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-84 2nd '8S 27-Mar-8S 3rd '8S lS-Jul-8S 4th '8S 09-0ct-8S 2nd'8G 24-Mar-8G 3rd '8G lO-Jul-8G 4th '8G 18-Dec-8G 2nd '87 20-Apr-87 3rd '87 OS-Jun-87 4th '87 22-Dec-87 2nd '88 19-Apr-88 3rd '88 28-Jul-88 2nd '89 07-Apr-89 3rd '89 OG-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd '90 20-Jun-90 3rd '90 17-0ct-90 1st '91 10-Apr-91 2nd '91 ll-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 10-Jun-92 3rd '92 10-Jun-92 1st '93 13-Apr-93 2nd '93 2G-Jun-93 3rd '93 12-0ct-93 1st '94 11-May-94 2nd '94 19-Jul-94 3rd '94 28-Nov-94 1st '9S 11-Apr-9S 2nd'9S OG-Jul-9S 3rd '9S lS-Nov-9S 1st '9G 23-Apr-9G 2nd '9G * 31-Jul-9G 3rd '9G 14-Nov-9G 1st '97 21-Apr-97 3rd '97 OS-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 1G-Jun-98 4th '98 OS-Nov-98 2nd '99 lS-Apr-99 3rd '99 07-Jul-99 4th '99 02-Dec-99 2nd '00 21-Apr-00 2nd '00 22-Jun-00 Ra-226 VALUE (uCi/Kg) 3.90E-04 L40E-04 L31E-04 LGOE-04 2.G7E-OG 9.3GE-OS L12E-04 L09E-04 3.47E-04 S.G1E-04 LOSE-03 8.20E-OS L1SE-04 S.72E-04 S.01E-04 8.70E-04 S.90E-04 LGOE-04 2.lOE-04 4.S0E-04 3.20E-OS S.GOE-04 LSOE-04 G.00E-04 2.GOE-04 L80E-04 LGOE-04 L20E-04 9.10E-OS 4.50E-04 3.GOE-OS LOOE-OS 7.90E-OS 3.70E-OS 3.00E-OS G.GOE-OS L80E-04 L71E-OS 2.40E-04 G.70E-OS LSOE-OS S.50E-OS S.20E-OS 3.00E-OS L10E-OS LlOE-OS 8.00E-OG <9.lOE-OS L80E-OS S.70E-OS 2.00E-04 G.03E-OS 2.30E-OS LSOE-04 L20E-OG Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (1.0E-06) LOE-OS S.OE-08 LlOE-03 LOE-04 LOE-OG LOE-OS S.OE-08 G.80E-04 8.0E-OS LOE-OG L3E-OS LOE-OG 4.90E-04 7.0E-OS 8.0E-OS LOE-OS S.OE-08 8.00E-04 L7E-04 1.0E-07 L1E-OG LOE-OG L08E-04 9.0E-OG 1.0E-OS G.2E-OG 8.0E-09 4.97E-04 9.3E-OS 1.0E-04 L2E-OS G.OE-OG L84E-04 L2E-OS LOE-OG 8.0E-OG 4.0E-OG 7.80E-04 G.2E-OS G.OE-OS L2E-OS 2.0E-09 3.7SE-03 LGE-04 4.0E-08 2.0E-04 2.0E-07 7.82E-03 3.3E-04 7.0E-08 3.0E-OS 2.0E-OG 3.22E-03 L4E-04 2.0E-OS 7.0E-OG 3.0E-OG 7.70E-04 L3E-04 2.0E-04 LOE-OS 3.0E-OG S.lOE-04 3.0E-OS 2.0E-OS 2.1E-OS 4.0E-OG 2.49E-03 LOE-04 LOE-OS L3E-OS 3.0E-OG LS7E-03 L7E-03 2.0E-04 S.OE-OS 3.0E-OG G.80E-04 3.0E-OS 3.0E-OG 7.0E-OS S.OE-08 LSOE-03 LOE-04 LOE-OG 3.0E-OS S.OE-08 9.50E-04 4.0E-OS LOE-OG 4.0E-OS S.OE-08 L70E-03 LOE-04 LOE-OG 7.0E-OS S.OE-08 L40E-03 LOE-04 LOE-OG 2.2E-OS S.OE-08 LSOE-04 4.4E-04 LOE-OG 4.0E-OS *** LlOE-03 LOE-Ol *** 2.0E-OS *** 2.30E-04 2.0E-OS *** S.OE-OS 7.0E-OG 2.04E-03 7.0E-OS l.4E-OS 3.0E-OS 4.0E-OG 3.30E-04 2.0E-OS 2.2E-OS 2.0E-OS S.OE-08 3.20E-04 2.0E-OS LOE-OG 2.0E-OS S.OE-08 3.30E-04 2.0E-OS LOE-OG 2.0E-OS S.OE-OG 3.00E-04 2.0E-OS LOE-OG loGE-OS 2.0E-07 L90E-04 2.0E-OS 2.0E-07 4.0E-OS S.OE-08 L09E-03 S.OE-OS LOE-OG LOE-OS 2.0E-OG LSOE-04 2.0E-OS LOE-OS 7.0E-OG 2.0E-07 7.S0E-OS 2.0E-OS LOE-OG 3.5E-OS 3.0E-OG 7.lOE-04 7.0E-OS 2.0E-OS 2.2E-OS 3.0E-OG 2.80E-04 3.0E-OS 2.0E-OS loSE-OS 3.0E-OG 4.30E-OS 3.5E-OS 2.0E-OS 2.7E-OS 3.0E-OG S.30E-04 G.OE-OS 2.0E-OS 4.0E-OS 3.0E-OS 4.40E-04 G.OE-OS 2.0E-04 L2E-OG 9.0E-08 3.00E-OS G.1E-OG 4.SE-OG loSE-OS L7E-07 L70E-04 L1E-OS 8.3E-07 S.4E-OG LGE-07 L40E-04 L3E-OS . 7.9E-07 LSE-OG LSE-07 S.lOE-OS 4.5E-OG 7.GE-07 S.OE-OG L8E-07 G.70E-OS LOE-OS 8.8E-07 2.5E-OG LSE-07 3.20E-OS 4.5E-OG L8E-07 2.5E-OG L8E-07 L40E-04 7.1E-OG 9.3E-07 4.7E-07 L2E-07 4.10E-OS 3.GE-OG G.IE-07 4.3E-07 L3E-07 2.lOE-OS 7.3E-07 G.7E-07 L2E-OG S.GE-07 L40E-04 4.GE-OG L1E-07 9.1E-OS 9.1E-OS <4.S0E-04 4.SE-04 4.5E-04 L2E-OG G.3E-08 4.00E-OS L8E-OG 3.2E-07 LOE-OG 8.2E-08 8.70E-OS S.OE-OG 4.1E-07 3.0E-OG 1.2E-07 3.00E-04 LOE-OS G.OE-OS L4E-OG 8.3E-08 L40E-04 4.7E-OG 4.2E-07 LOE-OG 2.3E-07 2.lOE-OS LOE-OG LIE-OG 3.0E-OG L2E-07 LGOE-04 8.0E-OG S.9E-07 LOE-07 2.8E-07 LGOE-04 LOE-OS L4E-OG 4th '00 21-0ec-00 L60E-06 L1E-06 3.7E-07 S.lOE-OS S.OE-06 L9E-06 1st '01 30-Apr-Ol LOOE-06 LOE-07 2.4E-07 <L2E-06 LOE-07 2.4E-07 2nd '01 14-Jun-Ol 2.30E-06 2.0E-07 9.9E-OS 3.S0E-06 2.0E-07 S.OE-07 4th '01 17-0ec-Ol 9.lOE-06 2.4E-06 L2E-07 3.57E-OS 3.0E-06 6.0E-07 1st '02 07-May-02 3.30E-OS LSE-06 7.6E-07 4.50E-OS 2.6E-06 LOE-OS 2nd '02 07-Jul-02 S.5SE-OS 2.SE-06 7.6E-07 S.31E-OS 3.9E-06 LOE-OS 4th '02 lS-0ec-02 7.7SE-OS 3.6E-06 7.6E-07 L29E-04 6.2E-06 LOE-OS 1st '03 21-Mar-03 9.10E-06 L3E-06 3.6E-07 L13E~OS L6E-06 3.4E-06 2nd '03 1O-Jun-03 2.50E-OS L3E-06 3.6E-07 3.26E-06 2.0E-06 7.4E-OS 4th '03 20-Nov-03 S.70E-OS 3.5E-06 LSE-07 4.0SE-OS S.SE-06 S.3E-07 1st '04 OS-Apr-04 9.3SE-OS 3.7E-06 L1E-07 S.SSE-OS 3.0E-06 S.5E-07 2nd '04 12-Jun-04 S.63E-OS 3.4E-06 LSE-07 6.42E-OS S.9E-06 9.0E-07 4th '04 30-Nov-04 S.41E-OS S.50E-06 2.00E-OS 2.4SE-04 L40E-OS 3.00E-07 1st 'OS 21-Apr-OS S.60E-OS 3.00E-06 L40E-07 S.SOE-OS 4.00E-06 6.90E-07 2nd '05 13-Jun-OS 9.lOE-06 LSOE-06 LSOE-07 Ll0E-OS L20E-OS 9.00E-07 4th 'OS 10-Nov-OS 6.00E-OS 3.00E-06 LlOE-10 L70E-06 6.40E-07 S.50E-1O 1st '06 03-Apr-06 S.OOE-OS S.00E-06 S.OOE-OS 3.40E-04 L20E-OS LOOE-06 2nd '06 16-Jun-06 4.lOE-OS 3.10E-06 S.OOE-OS L16E-04 6.10E-06 LOOE-06 4th '06 2S-Nov-06 L17E-04 4.60E-06 L90E-07 3.2SE-04 9.50E-06 9.50E-07 1st '07 30-Mar-07 9.70E-OS 4.40E-06 L90E-07 3.40E-04 S.70E-06 S.4-07 2nd '07 l-Jun-07 L30E-OS L60E-06 L90E-07 lo20E-04 6.60E-06 9.70E-07 4th '07 23-Nov-07 7.00E-OS S.20E-06 2.00E-07 S.00E-04 2.00E-OS L20E-06 1st 'OS 22-Apr-OS 3.6E-06 3.00E-06 S.20E-07 2.3E-04 L40E-OS LOOE-06 2nd 'OS lS-Jun-OS 3.2E-OS 3.20E-06 LSOE-06 6.9E-OS 3.50E-OS S.50E-OS 4th 'OS 12-0ec-OS 1st '09 2S-Apr-09 S.9E-04 L3SE-OS 1.S0E-06 3.4E-04 L30E-OS LSOE-06 2nd '09 17-Jun-09 L9E-OS L4SE-06 4.90E-07 3.6E-OS Ll0E-OS LSOE-OS 4th '09 lS-0ec-09 L7E-04 S.90E-06 4.SE-04 L20E-OS 1st '10 13-May-10 2.2E-04 7.20E-06 LlOE-06 1.9E-04 L90E-OS 2.90E-OS 2nd '10 lS-Jun-lO 6.SE-OS 3.40E-06 7.60E-07 lo4E-04 L90E-OS 2.90E-OS 4th '10 20-0ec-1O 2.3E-OS L70E-06 S.20E-07 loDE-OS LSOE-06 2.30E-06 2nd '11 23-Jun-11 2.4E-07 L4E-07 LSE-07 <2.9E-06 L7E-06 2.9E-06 2nd '12 ll-Apr-12 4.4E-OS L9E-06 3.6E-07 2.1E-04 2.0E-06 LOE-06 3rd'12 ll-Jun-12 2.2E-OS S.4E-07 L1E-07 lo3E-04 7.6E-06 S.9E-06 4th '12 06-Nov-12 3.1E-OS 4.SE-07 4.6E-OS 4.3E-04 3.7E-06 6.5E-07 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHWEST OF MILL SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0et-81 2nd '82 lS-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nov-82 2nd '83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-84 2nd'8S 27-Mar-8S 3rd '8S lS-Jul-8S 4th '8S 09-0et-8S 2nd '86 24-Mar-86 3rd '86 1O-Jul-86 4th '86 18-0ee-86 2nd '87 20-Apr-87 3rd '87 OS-Jun-87 4th '87 22-0ee-87 2nd '88 19-Apr-88 3rd '88 28-Jul-88 2nd '89 07-Apr-89 3rd '89 06-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd '90 20-Jun-90 3rd '90 17-0et-90 1st '91 1O-Apr-91 2nd '91 11-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 1O-Jun-92 3rd'92 1O-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd '93 12-0et-93 1st '94 ll-May-94 2nd '94 19-Jul-94 3rd '94 28-Nov-94 1st '9S ll-Apr-9S 2nd'9S 06-Jul-9S 3rd '9S lS-Nov-9S 1st '96 23-Apr-96 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd '97 OS-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 OS-Nov-98 2nd '99 lS-Apr-99 3rd '99 07-Jul-99 4th '99 02-0ee-99 2nd '00 21-Apr-00 Ra-226 VALUE (uCi/Kg) 2.73E-03 2.00E-04 l.04E-04 2.00E-OS 2.36E-06 8.58E-OS 1.19E-04 9.78E-OS 2.08E-04 6.0SE-04 l.lOE-04 6.10E-OS l.07E-04 8.86E-04 6.66E-04 S.20E-04 4.lOE-04 l.60E-04 3.60E-04 2.60E-04 3.10E-OS 6.20E-04 3.40E-04 S.10E-04 3.60E-04 l.70E-04 8.80E-OS 3.00E-04 3.lOE-04 S.00E-04 2.00E-OS 6.50E-06 l.20E-04 l.80E-OS S.20E-OS S.lOE-OS 1.20E-04 3.73E-OS 2.40E-04 8.40E-OS l.90E-OS l.20E-04 8.30E-OS 3.60E-OS 3.30E-OS S.40E-06 8.90E-06 <9.20E-OS < 6.50E-08 4.20E-OS 6.20E-OS S.4SE-OS l.10E-04 3.70E-OS Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (1.OE-06) S.OE-OS S.OE-08 7.lOE-03 3.0E-04 l.OE-06 l.OE-OS S.OE-08 8.30E-04 S.OE-OS l.OE-06 9.0E-06 7.0E-06 6.40E-04 S.OE-OS 4.0E-OS l.OE-OS S.OE-08 2.20E-04 9.0E-OS l.OE-07 9.5E-07 l.OE-06 8.00E-OS l.OE-OS l.OE-OS l.4E-OS 2.0E-08 3.53E-04 l.9E-OS l.OE-OS l.lE-OS S.OE-06 1.58E-04 l.3E-OS l.OE-OS 7.0E-06 2.0E-06 2.16E-03 3.4E-04 3.0E-04 l.OE-OS 3.0E-09 l.60E-03 7.0E-OS 3.0E-08 l.6E-04 2.0E-07 2.58E-03 l.lE-04 3.0E-08 8.0E-06 3.0E-06 8.63E-04 4.2E-OS 3.0E-OS 6.0E-06 2.0E-06 S.40E-04 S.OE-OS S.OE-OS 6.0E-06 2.0E-06 3.80E-04 3.0E-OS 2.0E-OS l.8E-OS 2.0E-06 4.40E-03 l.9E-04 3.0E-OS l.8E-OS 3.0E-06 4.78E-03 2.1E-04 6.0E-OS l.OE-04 3.0E-06 l.70E-03 l.OE-04 6.0E-OS l.OE-04 S.OE-08 l.60E-03 l.OE-04 l.OE-06 3.0E-OS S.OE-08 S.SOE-04 4.0E-OS l.OE-06 S.OE-OS S.OE-08 l.80E-03 l.OE-04 l.OE-06 S.OE-OS S.OE-08 l.90E-03 l.OE-04 l.OE-06 l.9E-OS S.OE-08 l.60E-04 4.0E-OS l.OE-06 S.OE-OS *** l.70E-03 l.OE-04 *** 3.0E-OS *** 7.40E-04 3.0E-OS *** 6.0E-OS 7.0E-06 l.00E-03 7.0E-OS l.4E-OS 3.0E-OS 4.0E-06 4.80E-04 2.0E-OS 2.2E-OS 2.0E-OS S.OE-08 3.20E-04 2.0E-OS l.OE-06 l.6E-OS S.OE-08 2.90E-04 2.0E-OS l.OE-06 3.0E-OS S.OE-06 4.10E-04 2.0E-OS l.OE-06 3.0E-OS 2.0E-07 4.70E-04 2.0E-OS 2.0E-07 4.0E-OS S.OE-08 l.SOE-03 l.OE-04 1.0E-06 8.0E-06 2.0E-06 9.60E-OS l.4E-OS 1.0E-OS 6.0E-06 2.0E-06 l.20E-04 2.0E-OS 1.0E-06 4.0E-OS 3.0E-06 l.21E-03 8.0E-OS 2.0E-OS l.7E-OS 3.0E-06 2.lOE-04 3.0E-OS 2.0E-OS l.9E-OS 3.0E-06 l.70E-OS 3.6E-OS 2.0E-OS 2.3E-OS 3.0E-06 7.lOE-04 6.0E-OS 2.0E-OS l.OE-OS 3.0E-OS 9.80E-04 l.6E-04 2.0E-04 l.6E-06 8.4E-08 7.80E-OS 7.1E-06 4.2E-07 l.5E-OS l.7E-07 2.60E-04 l.3E-OS 8.3E-07 6.1E-06 l.SE-07 l.20E-04 l.lE-OS 7.5E-OS l.SE-06 l.4E-07 4.50E-OS 4.3E-06 7.2E-07 6.8E-06 l.4E-07 l.OOE-OS S.8E-06 7.1E-07 3.3E-06 l.9E-07 6.80E-OS 6.3E-06 l.8E-07 2.5E-06 l.6E-07 8.50E-OS S.6E-06 8.4E-07 2.3E-06 l.7E-07 4.40E-OS 4.8E-06 8.4E-07 3.5E-07 l.6E-07 3.20E-OS 9.0E-07 7.8E-07 7.2E-07 S.4E-07 3.40E-04 6.7E-06 l.lE-07 9.2E-OS 9.2E-OS <4.60E-04 4.6E-04 4.6E-04 6.SE-08 6.5E-08 <3.20E-07 3.2E-07 3.2E-07 l.OE-06 l.lE-07 l.70E-04 l.OE-OS S.5E-07 l.OE-06 l.OE-07 l.40E-04 7.0E-06 LOE-07 l.4E-06 8.3E-08 9.20E-OS 4.0E-06 4.2E-07 3.0E-06 2.2E-07 2.80E-OS l.OE-06 l.lE-06 l.OE-06 2.4E-07 2.70E-04 l.OE-OS l.2E-06 2nd '00 22-Jun-00 2.90E-OS 1.0E-06 3.3E-07 2.BOE-04 2.0E-OS 1.7E-06 4th '00 21-0ec-00 2.30E-06 1.4E-06 3.7E-07 3.30E-04 S.OE-OS 1.9E-06 1st '01 30-Apr-Ol 2.10E-OS 1.0E-06 1.SE-07 <7.6E-07 N/A 7.6E-07 2nd '01 14-Jun-Ol 1.30E-06 4.0E-OB 1.2E-07 1.BOE-06 3.0E-OB S.9E-07 4th '01 17-0ec-Ol 3.70E-OS 7.67E-07 B.30E-OB 6.72E-OS 2.62E-06 6.00E-07 1st '02 07-May-02 4.90E-OS 2.40E-06 7.60E-07 1.2BE-04 S.61E-06 1.00E-OS 2nd '02 07-Jul-02 B.BBE-OS 4.32E-06 7.60E-07 B.33E-OS 4.32E-06 1.00E-OS 4th '02 lS-0ec-02 1.S0E-04 6.2E-06 7.60E-07 3.16E-04 1.07E-OS 1.0E-OS 1st '03 21-Mar-03 S.OOE-OS 3.4E-06 2.71E-06 <4.2e-6 4.20E-06 2nd '03 lD-Jun-03 S.60E-OS 2.0E-06 4.lDE-07 1.BBE-04 S.14E-06 B.2E-OB 4th '03 20-Nov-03 3.20E-04 B.2E-06 1.70E-07 4.B9E-04 1.2SE-OS B.3E-07 1st '04 OB-Apr-04 6.29E-OS 4.1E-06 2.00E-07 1.94E-OS 4.00E-06 1.0E-06 2nd '04 12-Jun-04 6.51E-OS 3.4E-06 1.30E-07 1.B7E-OS 3.90E-06 6.SE-07 4th '04 30-Nov-04 7.50E-OS 4.6E-06 2.0E-OB 4.4SE-04 1.40E-OS 3.0E-07 1st 'OS 21-Apr-OS 4.90E-OS 2.70E-06 1.30E-07 1.27E-04 4.BOE-06 6.S0E-07 2nd '05 13-Jun-OS 2.30E-OS 2.10E-06 1.S0E-07 4.70E-OS S.lDE-06 7.60E-07 4th 'OS 10-Nov-OS 7.40E-OS 3.S0E-06 1.20E-lD 2.40E-06 B.lDE-OB S.BOE-lO 1st '06 03-Apr-06 1.00E-04 6.00E-06 S.OOE-OB 6.S4E-04 1.S0E-OS 1.00E-06 2nd '06 16-Jun-06 9.S0E-OS S.90E-06 S.OOE-OB 4.4BE-04 1.40E-OS 1.00E-06 4th '06 2B-Nov-06 B.13E-OS 4.10E-06 2.20E-07 3.2SE-04 1.12E-06 1.00E-OS 1st '07 30-Mar-07 4.30E-OS 2.60E-06 1.70E-07 2.64E-04 7.20E-06 B.60E-07 2nd '07 l-Jun-07 S.10E-OS 3.20E-06 2.30E-07 S.30E-04 1.40E-06 1.20E-06 4th '07 23-Nov-07 7.30E-OS 6.6E-06 S.OE-OB 7.00E-04 2.20E-OS 1.lOE-06 1st 'OB 22-Apr-OB 2.BE-06 2.BE-06 7.20E-07 4.40E-04 2.0E-OS 1.0E-06 2nd'OB lB-Jun-OB 3.2E-06 3.3E-06 1.BOE-06 1.40E-04 3.3E-OS S.5E-OS 4th 'OB 12-0ec-OB 7.3E-OS 3.2E-06 7.40E-07 4.40E-04 2.SE-OS 3.2E-OS 1st '09 2B-Apr-09 S.3E-OS 3.6E-06 1.lDE-06 1.90E-04 l.5E-OS 2.2E-OS 2nd '09 17-Jun-09 2.3E-OS 1.6E-OS S.2E-07 4.30E-OS 1.00E-OS 1.7E-OS 4th '09 lB-Oec-09 S.50E-OS 3.50E-06 3.0E-04 1.lOE-OS lst'lO 13-May-l0 1.9E-04 6.lOE-06 9.40E-07 S.lE-04 2.40E-OS 3.lOE-OS 2nd'lO lB-Jun-lO 2.3E-OS 2.00E-06 7.70E-07 B.3E-OS 1.BOE-OS 2.90E-OS 4TH'lO 20-0ec-lO B.6E-06 9.lOE-07 3.90E-07 1.1E-07 6.BOE-07 1.lOE-06 2nd '11 23-Jun-11 2.1E-07 1.20E-07 1.40E-07 <2.2E-06 1.30E-06 2.20E-06 2nd '12 l1-Apr-12 1.SE-OS 9.S0E-07 2.60E-07 <7.0E-07 6.00E-07 1.00E-06 3rd'12 11-Jun-12 B.3E-06 S.40E-07 1.20E-07 1.4E-04 B.30E-06 6.50E-06 4th '12 06-Nov-12 2.3E-OS 4.lOE-07 7.71E-OB 4.6E-04 3.B3E-06 6.1BE-07 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this penod WHITE MESA MILL FORAGE RADIONUCLIDE DATA SOUTHWEST OF MILL SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd '82 lS-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nov-82 2nd '83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-84 2nd'8S 27-Mar-8S 3rd '8S lS-Jul-8S 4th '8S 09-0ct-8S 2nd '86 24-Mar-86 3rd '86 10-Jul-86 4th '86 18-0ec-86 2nd '87 20-Apr-87 3rd '87 OS-Jun-87 4th '87 22-0ec-87 2nd '88 19-Apr-88 3rd '88 28-Jul-88 2nd '89 07-Apr-89 3rd '89 06-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd '90 20-Jun-90 3rd '90 17-0ct-90 1st '91 lO-Apr-91 2nd '91 ll-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 lO-Jun-92 3rd '92 lO-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd '93 12-0ct-93 1st '94 ll-May-94 2nd '94 19-Jul-94 3rd '94 28-Nov-94 1st '9S ll-Apr-9S 2nd'9S 06-Jul-9S 3rd '9S lS-Nov-9S 1st '96 23-Apr-96 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd '97 OS-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 OS-Nov-98 2nd '99 lS-Apr-99 3rd '99 07-Jul-99 4th '99 02-0ec-99 2nd '00 21-Apr-00 Ra-226 VALUE (uCi/Kg) 9.S0E-04 3.00E-OS 1.37E-OS 3.40E-04 1.7SE-OS 7.13E-04 S.39E-OS 6.40E-OS 8.27E-OS 2.72E-04 4.73E-04 6.60E-OS 2.83E-04 1.S7E-04 3.78E-04 2.60E-04 4.lOE-04 2.90E-04 1.80E-04 2.30E-04 1.S0E-04 3.10E-04 1.30E-04 4.30E-04 2.50E-04 1.lOE-04 6.10E-OS 3.40E-OS 8.00E-OS 6.50E-OS 1.60E-OS 1.90E-OS 1.60E-OS 2.60E-OS 3.00E-OS 3.10E-OS 2.00E-OS 1.7SE-OS 1.00E-04 1.70E-OS 6.40E-06 2.30E-OS 4.20E-OS 2.lOE-OS S.SOE-06 S.30E-06 2.50E-OS <7.90E-OS 3.60E-07 4.30E-OS 2.40E-OS 2.23E-OS 1.50E-04 1.00E-04 Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (1.OE-06) 2.0E-OS S.OE-08 1.S0E-04 1.0E-OS 1.0E-06 3.0E-06 S.OE-08 1.S0E-04 2.0E-OS 1.0E-06 3.0E-06 3.0E-06 3.80E-04 4.0E-OS 4.0E-OS 2.0E-OS S.OE-08 3.68E-03 2.7E-04 1.0E-07 3.0E-06 2.0E-06 7.92E-04 4.0E-06 2.0E-OS 7.3E-OS 9.0E-08 2.51E-03 3.0E-04 3.0E-04 4.SE-06 2.0E-06 6.88E-04 4.3E-OS 4.0E-OS 7.0E-06 4.0E-06 1.20E-03 1.0E-04 4.0E-OS 6.3E-06 3.0E-09 1.80E-03 1.0E-04 9.0E-08 1.SE-04 2.0E-07 4.70E-03 7.2E-04 3.0E-07 1.6E-07 3.0E-06 7.07E-04 3.6E-OS 3.0E-OS 7.0E-06 4.0E-06 4.90E-04 3.0E-OS 3.0E-OS 2.0E-OS 7.0E-06 1.S0E-03 1.0E-04 7.0E-OS 1.0E-OS 4.0E-06 4.14E-03 1.8E-04 3.0E-OS 1.0E-OS 2.0E-06 1.6SE-02 7.0E-04 1.0E-04 2.0E-OS 2.0E-06 1.70E-03 1.0E-04 1.0E-04 7.0E-OS S.OE-08 2.20E-03 1.0E-04 1.0E-06 4.0E-OS S.OE-08 7.50E-04 S.OE-OS 1.OE-06 3.0E-OS S.OE-08 2.40E-03 1.0E-04 1.0E-06 S.OE-OS S.OE-08 2.90E-03 1.0E-04 1.0E-06 3.0E-OS S.OE-08 4.30E-03 2.0E-04 1.0E-06 4.0E-OS *** 4.20E-03 1.0E-04 *** 2.0E-OS *** 1.S0E-03 1.0E-04 *** S.OE-OS l.4E-OS 3.50E-03 1.4E-04 2.7E-OS 3.0E-OS S.OE-06 2.39E-03 S.OE-OS 2.5E-OS 2.0E-OS S.OE-08 6.60E-04 3.0E-OS 1.0E-06 1.4E-OS S.OE-08 6.10E-04 3.0E-OS 1.0E-06 1.1E-OS S.OE-06 2.20E-04 1.0E-OS 1.0E-06 6.0E-06 2.0E-07 1.20E-04 1.0E-OS 2.0E-07 l.4E-OS S.OE-08 9.10E-04 S.OE-OS 1.0E-06 7.0E-06 2.0E-06 3.20E-04 2.0E-OS 1.0E-OS 1.0E-OS 2.0E-07 2.20E-04 2.0E-OS 1.0E-06 1.8E-OS 3.0E-06 7.60E-04 6.0E-OS 2.0E-OS 2.0E-OS 3.0E-06 3.40E-04 3.0E-OS 2.0E-OS 1.4E-OS 3.0E-06 O.OOE+OO 3.0E-OS 2.0E-OS 1.6E-OS 3.0E-06 4.20E-04 6.0E-OS 2.0E-OS S.OE-06 3.0E-OS 3.90E-04 8.0E-OS 2.0E-04 1.7E-06 7.6E-08 1.30E-04 7.8E-06 3.8E-07 9.0E-06 1.5E-07 2.60E-04 1.2E-OS 7.4E-07 1.SE-06 1.6E-07 1.60E-04 l.5E-OS 8.1E-07 6.0E-07 1.4E-07 4.40E-OS 4.2E-06 7.0E-07 2.2E-06 1.7E-07 6.60E-OS 9.6E-06 8.3E-07 2.2E-06 1.7E-07 1.00E-04 6.7E-06 1.8E-07 2.0E-06 1.6E-07 1.90E-04 7.3E-06 8.2E-07 4.2E-07 1.4E-07 3.30E-OS 3.9E-06 7.0E-07 3.2E-07 1.3E-07 1.90E-OS 6.9E-07 6.3E-07 9.SE-07 S.9E-07 1.30E-04 4.7E-06 1.2E-07 7.9E-OS 7.9E-OS <3.90E-04 3.9E-04 3.9E-04 1.4E-07 3.3E-08 <1.7E-07 1.7E-07 1.7E-07 1.0E-06 7.6E-08 2.50E-04 1.0E-OS 3.8E-07 1.0E-06 1.2E-07 1.70E-04 8.0E-06 6.2E-07 8.6E-07 1.2E-07 2.30E-04 7.0E-06 S.9E-07 3.0E-06 2.0E-07 1.70E-OS 1.0E-06 1.0E-06 2.0E-06 1.2E-07 1.lOE-04 7.0E-06 6.1E-07 2nd '00 22-Jun-00 L30E-06 LOE-07 2.4E-07 2.00E-04 LOE-OS L2E-06 4th '00 21-0ec-00 L20E-06 9.0E-07 2.4E-07 L20E-04 3.0E-OS L2E-06 1st '01 30-Apr-01 L80E-06 LOE-07 L7E-07 <8.3E-07 N/A 8.3E-07 2nd '01 14-Jun-01 2.60E-06 2.0E-07 9.9E-08 L10E-06 2.0E-08 S.OE-07 4th '01 17-0ec-01 2.63E-06 4.6E-OS L2E-07 9.40E-OS 3.7E-06 6.0E-07 1st '02 07-May-02 3.50E-OS 2.2E-06 7.6E-07 L36E-04 S.6E-06 LOE-OS 2nd '02 07-Jul-02 4.02E-OS 2.3E-06 7.6E-07 7.04E-OS 4.1E-06 LOE-OS 4th '02 1S-0ec-02 8.lOE-OS 3.9E-06 7.6E-07 2.87E-04 8.SE-06 LOE-OS 1st '03 21-Mar-03 3.70E-OS 2.6E-06 2.4E-06 2.69E-OS 2.0E-06 3.7E-06 2nd '03 lO-Jun-03 L30E-OS LOE-06 S.2E-07 <LOOE-07 LOE-07 4th '03 20-Nov-03 L60E-04 L3E-OS L2E-07 L42E-04 6.4E-06 S.9E-07 1st '04 08-Apr-04 1.40E-04 7.7E-06 L1E-07 6.10E-06 2.7E-06 S.SE-07 2nd '04 12-Jun-04 6.51E-OS 3.2E-06 l.SE-07 S.27E-OS 4.9E-06 7.6E-07 4th '04 30-Nov-04 8.40E-OS S.7E-06 3.0E-08 3.39E-04 L6E-OS 3.0E-07 1st 'OS 21-Apr-OS L70E-OS L6E-06 L3E-07 4.50E-OS 3.SE-06 6.5E-07 2nd '05 13-Jun-OS 1.50E-OS L6E-06 1.4E-07 7.00E-OS S.1E-06 6.9E-07 4th 'OS 10-Nov-OS 3.80E-OS 2.1E-06 8.6E-10 L20E-06 4.8E-08 4.3E-10 1st '06 03-Apr-06 LOOE-04 6.0E-06 S.OE-08 3.30E-04 L1E-OS LOE-06 2nd '06 16-Jun-06 3.40E-OS 2.5E-06 S.OE-08 L37E-04 6.0E-06 1.0E-06 4th '06 28-Nov-06 7.31E-OS 3.20E-06 L60E-07 2.98E-04 8.50E-06 8.20E-07 1st '07 30-Mar-07 3.00E-OS 2.20E-06 L70E-07 3.20E-04 7.90E-06 8.40E-07 2nd '07 1-Jun-07 LlOE-04 4.60E-06 2.3-07 3.20E-04 LlOE-OS 1.10E-06 4th '07 23-Nov-07 S.60E-OS S.20E-06 S.00E-08 6.40E-04 L90E-OS LOOE-06 1st '08 22-Apr-08 3.20E-OS 2.30E-06 7.20E-07 2.30E-04 LSOE-OS LOOE-06 2nd '08 18-Jun-08 L2SE-OS 2.20E-06 L80E-06 S.OOE-OS 3.00E-OS 4.80E-03 4th '08 12-0ec-08 1st '09 28-Apr-09 2.60E-OS 2.90E-06 L40E-06 3.70E-OS LSOE-06 2.50E-OS 2nd '09 17-Jun-09 2.40E-OS L40E-06 3.90E-07 3.50E-OS 7.90E-06 L30E-OS 4th '09 18-0ec-09 3.1E-OS 2.30E-06 2.1E-04 8.40E-06 1st'lO 13-May-lO 2.0E-OS 2.10E-06 9.40E-07 S.6E-OS LSOE-OS 2.40E-OS 2nd '10 18-Jun-lO L1E-OS L30E-06 6.60E-07 7.8E-OS L60E-OS 2.50E-OS 4th'lO 20-0ec-10 6.7E-06 9.lOE-07 4.80E-07 8.0E-07 7.90E-07 L30E-06 2nd '11 23-Jun-11 <L7E-07 6.9E-08 L7E-07 <2.SE-06 LSE-06 2.5E-06 2nd '12 11-Apr-12 S.OE-06 6.0E-07 3.0E-07 <7.0E-07 7.0E-07 LOE-06 3rd'12 11-Jun-12 L9E-08 6.2E-08 L1E-07 <2.5E-07 L3E-06 2.2E-06 4th '12 06-Nov-12 loSE-OS 3.4E-07 4.3E-08 4.5E-04 4.0E-06 8.6E-07 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period mD I Laboratories LLC a member of The GEL Group INC PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 December 05,2012 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: Vegetation Analysis Work Order: 314963 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on November 09,2012. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4505. Purchase Order: DW16138 Enclosures Sincerely, Heather Shaffer Project Manager www.gel.com Energy Fuels Resources (USA), Inc. Vegetation Analysis SDG: 314963 Table of Contents Case Narrative ...................................................................................... 1 Chain of Custody and Supporting Documentation ............................... 3 Laboratory Certifications ...................................................................... 8 Radiological Analysis ......................................................................... 1 0 Sample Data Summary ............................................................... 16 Quality Control Data .................................................................. 20 Case Narrative December 05, 2012 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 314963 Sample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on November 09, 2012 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification: The laboratory received the following samples: Laboratory ID Client ID 314963001 North East 314963002 North West 314963003 South West Case Narrative: Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. Data Package: The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Heather Shaffer Project Manager Chain of Custody and Supporting Documentation Sheet 1 of1 CHAIN OF CUSTODY Samples Shipped to: GEL Laboratories Contact: ------------------------Garrin Palmer or David Turk Ph: 435 678 2221 2040 Savage Rd Charleston, South Carolina 29407 8palmer@denisonmines.com dturk@denisonmines.com tholl iday@denisonmines.com Chain of Custody/Sampling Analysis Request P . t rOJec S amp ers N ame S amp ers S· t Igna ure Late fall Vegetation ... " ........ ./' (Ltf'..Ft!.(". ~:< ;: 2012 Tanner Holliday Date Time Sample 10 Collected Collected Laboratory Analysis Requested North East 11/6/2012 900 RA 226, PB 210 North West 11/6/2012 930 RA 226, PB 210 South West 11/6/2012 1015 RA 226, PB 211 Please notify Garrin Palmer or Tanner Holliday of Reciept tempature on these samples Immediately! Thank you. Relinquished By:(~ignature) ., .. ""\ .. / / .", ,,;/ "...... ..) :k./7/<(:~·C l:">·:/<·~:·~~;~:"l>~~~:;~-···"· '~I Relinquished By:(Signature) Date/Time Received By:(Signature) 11/7/2012 1100 Da~/Time \I~'l'" 2. 2 2a Daily check performed and passed on IR temperature gun? 3 Chain of custody documents included shipment? 4 Sample containers intact and sealed? 5 Samples requiring chemical preservation at proper pH? 6 VDA vials free of heads pace (defined as < 6mm bubble)? 7 Are Encore containers present? 8 Samples received within holding time" 9 Sample ID's on CDC match lO's on bottles? 10 Date & time on CDC match date & on bottles? II Number of containers received match number indicated on COC? 12 Are sample containers identifiable as GEL provided? 13 CDC form is properly signed in relinquished/received sections? 14 Carrier and tracking number. Comments (Use Continuation Fonu if needed): SAMPLE RECEIPT & REVIEW FORM Seals broken Damaged container Leaking (describe) Preservation Method: Ice bags Blue ice Dry ice None Other (describe) *all temperatures are recorded in Celsius Device Serial #: ISec)ondlaryTemperalure Device Serial # (If Applicable): Circle Applicable: Seals broken Damaged container Leaking container Other (describe) Sample ID's, containers affected and observed pH: Sample ID's and containers affected: (If yes, immediately deliver to les laboratory) Sample lOts and containers affected: Sample ID's affected: FedEx Air FedEx Ground Circle Applicable: UPS Field Services Courier Other -...... G9qb :t5~Lf > qi?~b .q:,q q<i Co +-2.3 PM (or PMA) review: Initials _....:"{):....' . .:..' ..:::0:..1! _____ Date \l _\ (Q .,' 2.. Page -L of-L- GEL Laboratories LLC -Login Review Report Report Date: 05-DEC-12 Work Order: 314963 Page 1 of 2 GEL Work Order/SDG: 314963 Client SDG: 314963 Project Manager: Project Name: Purchase Order: Package Level: EDD Format: Heather Shaffer DNMI00101 Vegetation Analysis DW16138 LEVEL3 EIM_DNMI GELID Client Sample 10 Client Sample Desc. 314963001 North East 314963002 North West 314963003 South West Client Sample 10 Status Tests/Methods -001 North East REVW GFPC, Total Alpha Radium, solid REVW GFPC, Pb210, Solid -002 North West REVW GFPC, Total Alpha Radium, solid REVW GFPC, Pb210, Solid -003 South West REVW GFPC, Total Alpha Radium, solid REVW GFPC, Pb210, Solid Work Order Due Date: 13-DEC-12 Package Due Date: EDD Due Date: Due Date: HXS1 10-DEC-12 13-DEC-12 13-DEC-12 Collector: C Prelogin #: 20121197700 Project Workdef ID: 1310529 SOG Status: Closed logged by: Collect Date & Time Receive Time # of Date & Time Zone Cont. Lab Matrix Fax Days to Due Date Process CofC# Prelog Lab Field Group QC QC 06-NOV-1209:00 09-NOV-12 09:20 0 06-NOV-1209:30 09-NOV-12 09:20 0 06-NOV-1210:15 09-NOV-12 09:20 0 Product Reference Fax Date PM Comments Prep: Please use 20009 of sample to dry Prep: Please use 20009 of sample to dry Prep: Please use 20009 of sample to dry VEGETATION VEGETATION VEGETATION Cooler Seal Undisturbed Temperature (C) Cooler Seal Undisturbed Temperature (C) Cooler Seal Undisturbed Temperature (C) 30 30 30 Aux Data y 23 y 23 y 23 Receive Codes Product: GFC_PBS VVorkdeflD: 1310600 In Product Group? No Group Name: Group Reference: Method: DOE RP280 Modified Product Description: GFPC, Pb210, Solid Samples: 001, 002, 003 Parmname Check: All parmnames scheduled properly CAS # Parmname 14255-04-0 Lead-210 Client RDL or PQL& Unit .000001 Reporting Units uCi/kg Path: Standard Product Reference: Moisture Correction: "As Received" Parm Included Included Custom Function in Sample? in QC? List? REG Y Y Yes GEL Laboratories LLC -Login Review Report Product: GFCTORAS Workdef 10: 1310679 Method: EPA 900.1 Modified Product Description: GFPC, Total Alpha Radium, solid Samples: 001,002,003 Parmname Check: All parmnames scheduled properly CAS # Parmname Total Radium In Product Group? No Action Product Name Description Contingent Tests Login Requirements: Requirement Group Name: Group Reference: Report Date: 05-DEC-12 Work Order: 314963 Page 2 of 2 Path: Standard Product Reference: Moisture Correction: "As Received" Client RDL or PQL & Unit Reporting Parm Included Included Custom Units Function in Sample? in QC? List? .00000005 uCi/kg REG Y Y Yes Samples Include? Comments Peer Review by: ___________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? _____ _ Laboratory Certifications List of current GEL Certifications as of 05 December 2012 State Certification Arkansas 88-0651 CLIA 42D0904046 California NELAP 01151CA Colorado SCOOO12 Connecticut PH-0169 Delaware SCOOO12 DoD ELAP A2LA ISO 17025 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-12-00283,P330-12-00284 Georgia SCOOO12 Georgia SDW A 967 Hawaii SCOOO12 Idaho SCOOO12 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky 90129 Louisiana NELAP 03046 (AI33904) Louisiana SDW A LA120008 Maryland 270 Massachusetts M-SC012 Mississippi SCOOO12 Nevada SCOOO122011-1 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SCOOO12 New York NELAP 11501 North Carolina 233 North Carolina SDW A 45709 Oklahoma 9904 Pennsylvania NELAP 68-00485 Plant Material Permit PDEP-12-00260 South Carolina Chemistry 10120001 South Carolina Radiochemi 10120002 Tennessee TN 02934 TexasNELAP T104704235-12-7 UtahNELAP SCOOO12 Vermont VT87156 Virginia NELAP 460202 Washington C780-12 Wisconsin 999887790 Radiological Analysis Radiochemistry Case Narrative Energy Fuels Resources (DNMI) SDG314963 Method/Analysis Information Product: GFPC, Pb210, Solid Analytical Method: DOE RP280 Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1264113 Prep Batch Number: 1263219 Sample ID Client ID 314963001 North East 314963002 North West 314963003 South West 1202781968 Method Blank (MB) 1202781969 314963003(South West) Sample Duplicate (DUP) 1202781970 314963003(South West) Matrix Spike (MS) 1202781971 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-018 REV# 13. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Ouality Control (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 314963003 (South West). QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The blank result 1202781968 (MB) is greater than the MDC but less than the required detection limit. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Additional Comments The matrix spike, 1202781970 (South West), aliquot was reduced to conserve sample volume. Qualifier Information Manual qualifiers were not required. Method/Analysis Information Product: GFPC, Total Alpha Radium, solid Analytical Method: EPA 900.1 Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1264114 Prep Batch Number: 1263219 SampleID 314963001 314963002 314963003 1202781972 1202781973 1202781974 1202781975 Client ID North East North West South West Method Blank (MB) 314963001(North East) Sample Duplicate (DUP) 314963001(North East) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-010 REV# 14. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Ouality Control (OC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 314963001 (North East). QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The blank, 1202781972 (MB), did not meet the detection limit due to keeping the blank volume consistent with the other sample aliquots. All other samples met the detection limits. The sample and the duplicate, 1202781973 (North East) and 314963001 (North East) , did not meet the relative percent difference requirement; however, they do meet the relative error ratio requirement with value of2.7807. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis Samples were recounted due to high recovery. The recounts are reported. Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Additional Comments The matrix spike, 1202781974 (North East), aliquot was reduced to conserve sample volume. Qualifier Information Manual qualifiers were not required. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMI001 Energy Fuels Resources (USA), Inc. Client SDG: 314963 GEL Work Order: 314963 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the cRDL. Review/Validation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all eLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: 9l 0 c::...tLw eJ . IY. <... ( 4' ('j tt Date: 02 JAN 2013 Name: Heather McCarty Title: Analyst II Sample Data Summary GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: January 2, 2013 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Vegetation Analysis North East 314963001 Vegetation 06-NOV-12 09:00 09-NOV-12 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "As Received" Lead-21O 0.000426 +/-3.72E-06 GFPC, Total Alpha Radium, solid "As Received" Total Radium 3.lOE-05 +/-4.82E-07 The following Prep Methods were performed: Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: Method Description DOE RP280 Modified 2 EPA 900.1 Modified Surrogate/Tracer Recovery Test GFPC, Pb210, Solid "As Received" DL 6.52E-07 4.63E-08 Lead Carrier Barium Carrier GFPC, Total Alpha Radium, solid "As Received" RL 1.00E-06 5.00E-08 Analyst LYTl Project: Client ID: DNMIOOI01 DNMI001 Units DF Analyst Date Time Batch Method uCilkg uCilkg Date 11114/12 Result BXFl 01101113 BXFl 01102113 Time Prep Batch 0609 1263219 Analyst Comments Nominal Recovery% 101 122 1640 1264113 0743 1264114 Acceptable Limits (25%-125%) (25%-125%) 2 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: January 2, 2013 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Vegetation Analysis North West 314963002 Vegetation 06-NOV-12 09:30 09-NOV-12 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "As Received" Lead-21O 0.000459 +/-3.83E-06 GFPC, Total Alpha Radium, solid "As Received" Total Radium 2.34E-05 +/-4.IOE-07 The following Prep Methods were performed: Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: Method Description DOE RP280 Modified 2 EPA 900.1 Modified Surrogate/Tracer Recovery Test GFPC, Pb210, Solid "As Received" DL 6.18E-07 7.71E-08 Lead Carrier Barium Carrier GFPC, Total Alpha Radium, solid "As Received" RL 1.00E-06 5.00E-08 Analyst LYTl Project: Client ID: DNMIOOI0l DNMIOOI Units DF Analyst Date Time Batch Method uCi/kg uCi/kg Date 11114112 Result BXFl 01101113 BXFl 01101113 Time Prep Batch 0609 1263219 Analyst Comments Nominal Recovery% 100 124 1640 1264113 1634 1264114 Acceptable Limits (25%-125%) (25%-125%) 2 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: January 2, 2013 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Parameter Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel Vegetation Analysis South West 314963003 Vegetation 06-NOV-1210:15 09-NOV-12 Client Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Pb210, Solid "As Received" DL Lead-21O 0.000445 +/-4.0lE-06 8.57E-07 GFPC, Total Alpha Radium, solid "As Received" Total Radium 1.49E-05 +/-3.4lE-07 4.25E-08 The following Prep Methods were performed: Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed: Method Description DOE RP280 Modified 2 EPA 900.1 Modified Surrogate/Tracer Recovery Test Lead Carrier Barium Carrier GFPC, Pb21O, Solid "As Received" GFPC, Total Alpha Radium, solid "As Received" RL 1.00E-06 5.00E-08 Analyst LYTl Project: Client ID: DNMI00101 DNMI001 Units DF Analyst Date Time Batch Method uCi/kg BXF1 01/01/l3 1640 1264113 uCi/kg BXF1 01/01/l3 1634 1264114 Date Time Prep Batch 11114/12 0609 1263219 Result Analyst Comments Nominal Recovery% 96.6 123 Acceptable Limits (25%-125%) (25%-125%) 2 Quality Control Data GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Contact: Workorder: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Ms. Kathy Weinel 314963 Parmname NOM Sample Qual QC Rad Gas Flow Batch 1264113 QC1202781969 314963003 DUP Lead-21O 0.000445 Uncertainty +/-4.01E-06 QC1202781971 LCS Lead-210 0.00802 Uncertainty QC1202781968 MB Lead-210 Uncertainty QC1202781970 314963003 MS Lead-210 0.0244 0.000445 Uncertainty +/-4.01E-06 Batch 1264114 QC1202781973 314963001 DUP Total Radium 3.10E-05 Uncertainty +/-4.82E-07 QC1202781975 LCS Total Radium 0.000203 Uncertainty QC1202781972 MB Total Radium Uncertainty QC1202781974 314963001 MS Total Radium 0.000528 3.10E-05 Uncertainty +/-4.82E-07 Notes: The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product 0.000388 +/-3.63E-06 0.0081 +/-4.92E-05 U 8.06E-07 +/-4.56E-07 0.0242 +/-0.000142 2.48E-05 +/-4.08E-07 0.000237 +/-4.85E-06 U 5.66E-08 +/-4. 62E-08 0.000685 +/-1.20E-05 Units RPD% uCilkg 13.5 uCilkg uCilkg uCi/kg uCilkg 22.2* uCi/kg uCi/kg uCilkg A B BD C D F H For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Reoort Date: January 2, 2013 Page lof 2 REC% Range Anlst (0% -20%) BXFl 101 (75%-125%) 97.2 (75%-125%) (0% -20%) BXFI 117 (75%-125%) 124 (75%-125%) Date Ti 01/01/13 1 01/01113 1 01/01/13 1 01/01113 1 01/02/13 ( 12/30/12 1 01/02/13 ( 12/30/12 1 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 314963 Parmname NOM Sample Qual QC Units RPD% K Analyte present. Reported value may be biased high. Actual value is expected to be lower. L Analyte present. Reported value may be biased low. Actual value is expected to be higher. M M if above MDC and less than LLD M Matrix Related Failure N/A RPD or %Recovery limits do not apply. See case narrative Analyte concentration is not detected above the detection limit NI ND NJ Q R U Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the cRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification REC% Page 2 of 2 Ran~e Anlst UI UJ UL X Y Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier /\ h QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded N/ A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more. Date Ti /\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater tha five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. ATTACHMENT G STACK SAMPLE LABORATORY RESULTS Prepared for: Energy Fuels Resources- 6425 S Hwy 91 Blanding, Utah 84511 . Date of Report: . December 6, 2012 THIRD QUARTER RADIONUCLIDE EMISSIONS TEST CONDUCTED AT ENERGY FUELS RESOURCES NORTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE BLANDING, UTAH September 28-29, 2012 by: TETCO 391 East 620 South . American Fork, UT 84003 . Phone (801) 492-9106 Fax (801) 492-9.107 fax CERTIFICATION OF REPORT INTEGRITY TechnicarEmissions Testing Company (TETCO) certifies that this report represents the truth as . well as can be derived by the methods employed. Every effort was made to obtain accurate and . representative data and to comply With procedures set forth in the Federal Register. · 1Za. ¥iZ Kitchen Date: __ --'-/02_!4'--.~-.:.....!t_!_Z---_· _ .. --:--_ .. _. _. _ Reviewer: Dean Kitchen Reviewer: ____ ...... ~'"---'-. ...:::.~~. :;-.._.J:..~:"'-""::~_. __ Date: . / ~ -~ _..( 2--------------~--~--~~~~~-- ii TABLE OF CONTENTS Introduction Test Purpose .................... ~ ...................................................................................................... 1 Test Location and Type of Process ................................................................................................ 1 Test Dates .......................................................................................................... ~ ....................... 1 -Pollutants Tested and Methods Applied ... ~ ......................................................................................... 1 Test Participants ....... ' ............................................................. ~ .......................... -.................... ~ ... 2 Deviations from EPA Methods ................................................................................. · ..................... 2 Quality Assurance ............................................................................................ ; ....................... ~2 Summary of Results Emission Results ...................................................................................................................... · .. 3 ProcessData ..................... ~ .................................................... ~ ................................................. 3 Description of Collected Samples ... · .. ~ ....................................................................................... 3 Discussion of Errors or Irregularities .......................................... ~ ..... ~ ............................................... 3 Percent Isokinetics .......... ~ ............................................................ · .............................................. 4 Source Operation Process Control Devices Operation .............................. ~ ........................................................ 5 Process Representativeness ................................................................. ~ ..................................... 5 . . , Sampling and Analysis Procedures Sampling Port Location .......................................................................................................... 6 . Sampling Point Location ................................................................................. ~ ........ ~ ....•........ 6 Sampling Train Description ...... ~ ........................... ~ ....................................................................... 6 . Sampling and Analytical Procedures ..................... ; ........................................................ ~ ...... 7 Quality Assurance ................................................................................................................... 7 Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data . E: Calibration Procedures and Results F:' Related Correspondence iii I ) . Table I II III IV V Figure LIST OF TABLES PAGE :Nleasured Radionuclide Emissions ...................................................................................... 3 Percent Isokinetics ................................................................................................................ 4 Sampling P·oir'lt Location ....................................................................................................... 6 Complete Results, North Yellow CaJ<e Scrubber .............................................. Appendix A Complete Results, Yellow Cake Dryer Baghouse ........................................ ; .... Appendix A LIST OF FIGURES 1 Facility Schematic Representation North Yellow Cake Scrubber ........ ; ......... ~:. Appendix D .2 Facility Schematic Representation Yellow Cake Dryer Baghouse .................... Appendix D 3 Schematic of Method 51114 Sampling Train ........... ~ ... ~ ................................. ~ ... Appendix E iv INTRODUCTION Test Purpose This test project was conducted to determine the total radionuclide emissions from the North Yellow Cake Scrubber and the Y ellow ~Cake Dryer Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dscf). These tests were for U-Nat only. Test Location and Type of Process Energy Fuels Resources is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer .enclosures discharge into the Yellow Cake Dryer Baghouse .. The packaging enclosure also discharges into' the Yellow· Cake Dryer Baghouse. The North Yellow Cake (NYC) dryer was the only operating dryer at the time of the test. The South Yellow Cake dryer is currently not operational. The Grizzly Baghouse serves as the main dust control device for the raw ore unloading and conveying to the processing building. . . Stack schematics are shown as Figures 1 and 2 in Appendix D. Test Dates One test run was .completed onthe NYC Scrubber September 28, 2012 and one run on September 29th• One run· was completed on the YellowCake Dryer Baghouse September 28,2012. Pollutants Tested and Methods Applied The tests were a determination of radionuclide emissions in accordance with EPA Method 5/114. Test run filters and front wash residues were sent to Test America located in Richland, Washington for radionuclide analysis. Test Participants . Test Facility State Agency TETCO Garren Palmer None Dean Kitchen Jeff Graton Deviations From EPA Methods None Quality Assurance Doug Olsen Testing procedures and sample recovery techniques were according to those outlined in the Federal Register and the Quality Assurance Handbookfor Air Pollution Measurement Systems. 2 SUMMARY OF RESULTS Emission Results Table I presents the findings of the test in Curiesper dry standard cubic fo~t. Tables IV-VI in Appendix A have more detailed information . . Table I. Measured Radionuclide Emissions North Yellow Cake Scrubber Yellow Cake Dryer Baghouse Run # pCi/dscf pCilhr pCi/dscf pCi/hr 1 239.3 1.986E +07 33.7 6.168E+06 2 185.7 L619E+07 AVE 212.5 I 1.802E+07 33.7 6.168E+06 Process Data The process W9-S operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow, pressure drop readings (~p) were recorded and are found in Appendix D. "The Dryer Baghouse pressure drop readings (~p) were recorded and are found on the test run sheets. Production data will be submitted by Energy Fuels Resources. Description of Collected Samples The test filters for the North Yellow, Cake Scrubber were heavily covered with a white or pinkish white colored particulate. The front washes were clear in appearance. The test filters for theY ellow Cake Dryer Baghouse were lightly colored with a tan colored particulate. The front wash was clear in appearance. Discussion of Errors or Irregularities None 3 Percent Isokinetic Sampling Each test run was isokinetic within the ±1 0% of 100% criterion specified in the Federal Register. Isokinetic values for each test run are presented in Table II. Table II. Percent Isokinetic Run # 1 2 North Yellow Cake Yellow Cake Dryer Scrubber Baghouse 99 100 96 4 SOURCE OPERATION Process Control Devices Operation All process control devices were operated normally. Recorded sc:r:ubber water flow, pressure and baghouse ~p readings were recorded and are found on the test run sheets or in Appendix D. Process Representativeness The facility was operated normally. Production data was retained by El1:ergy Fuels Resources. 5 i i J SAMPLING AND ANALYSIS PROCEDURES Sampling Port" Location The inside diameter of the North Yellow Cake Scrubber stack is 18.0 inches. The two, four-inch diameter sample port are located 6.3 diameters (9.5 feet) downstream from the last disturbance - and 6.3 diameters (9.5 feet) upstream from the next disturbance. Figure 1 in Appendix D is a schem.atic of the stack. The inside diameter. of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch diameter sample ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sample port locations are depicted in Figure 2 in Appendix D. Sampling Point Location Table III shows the distance of each sampling point from the inside wall according to EP A Method 1; Each point is marked and identified with a wrapping of glass tape and numbered. These points are determined by measuring the distance from the inside wall. TableIII. Distance (inches) from Inside Wall Sample Point NYC Scrubber Dryer Baghouse 1 0.58 0.70 2 1.89 2.34 3 3.49 . 4.74 4 5.81 11.26 5 12.19 13.66 6 14.51 15.30 7 16.11 8 17.42 Sampling Train Description To determine the actu~lemissionratesfor this stack, 40CFR 60, Appendix A, Methods 1·j/114 were followed. 6 All sampling trains were made of inert materials, (Teflon, stainless steel and glass) to prevent interference of the sampled gas and particulate. The stack-analyzers used to conduct Methods 1- 5/114 are constructed to meet the specifications outlinedin the CFR. The temperature sensors are K-type thermocouples. Heater, vacuum and pitot line connections have been designed to be interchangeable with all units used by the tester. A 316 stainless steelprobe liner was used for the tests. Figure 4 in Appen~ix E is a sketch of the Methods 5/114 sampling train. Sample boxes were prepared for testing by following the prescribed procedures outlined in Methods 5/114. Sampling and Analytical Procedures All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 5/114. Quality Assurance All equipment setup, sampling procedures, sample recovery and equipment calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbook/or Air Pollution Measurement Systems. 7 APPENDIX A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence 8 APPENDIX A Table IV Complete Results, North Yellow Cake Scrubber TableV Complete Results, Yellow Cake Dryer Baghouse N omenc1ature Sample Equations A Symbol Date Filter # Begin End Pbm i1H Y Vm Tm -Vi1P Wtwc T t C p On CO2 O 2 N2 &CO Vmstd Vw Bws Xd Md Ms %1 Ts As Po Pbp Ps Os Oa Vs Curies Crad ERrad TABLE V COMPLETE RESULTS. PM ENERGY FUELS RESOURCES YELLOW CAKE DRYER BAG HOUSE Description Dimensions Run #1 Date 9/28/2012 6038 TimeTest Began 10:43 Time Test Ended 12:45 Meter Barometric Pressure In. Hg. Abs 24.55 Orifice Pressure Drop In. H2O 2.133 Meter Calibration Y Factor dimensionless 1.006 Volume Gas Sampled--Meter Conditions cf 113.314 Avg Meter Temperature of 90.6 Sq Root Velocity Head Root In. H2O 0.7506 Weight Water Collected Grams 22.2 Duration of Test Minutes 120 Pitot Tube Coefficient Dimensionless 0.84 Nozzle Diameter Inches 0.2515 Volume % Carbon Dioxide Percent 0.00 Volume % Oxygen Percent 20.90 Volume % Nitrogen and Carbon Monoxide Percent 79.10 Volume Gas Sampled (Standard) dscf 90.268 Volume Water Vapor scf 1.047 Fraction H20 in Stack Gas Fraction 0.011 Fraction of Dry Gas Fraction 0.989 Molecular Wt. Dry Gas Ib/lbmol 28.84 Molecular wt. Stack Gas Ib/lbmol 28.71 Percent Isokinetic Percent 99.9 Avg Stack Temperature of 109.1 Stack Cross Sectional Area Sq. Ft. 1.396 Stack Static Pressure In. H2O -0.47 Sample Port Barometric Pressure In. Hg. Abs 24.48 Stack Pressure In. Hg. Abs 24.445 Stack Gas Volumetric Flow Rate (Std) dsctin 3.05E+03 Stack Gas Volumetric Flow Rate (Actual) ctin 4.07E+03 Velocity of Stack Gas fpm 2.91 E+03 Radionuclides per sample pCi 3040.0 Concentration of Radionuclides pCi/dscf 33.6774 Emission Rate of Radionuclides pCi/hr 6.156E+06 Dryer Baghouse %1 = percent isokinetic, percent As = stack cross-sectional area (ft2) AS~P = see ~~P Stu = unit heat value (British thennal unit) Nomenclature Bws = fraction of water in stack gas (may have designation of "measured" or "saturated") "measured" represents measured moisture based upon sample volume and water collected "saturated" is a calculated value based upon stack pressure and temperature Co = average of initial and final system zero gas calibration bias checks (ppm, percent) Cavg = average gas concentration (as measured) CB = concentration of particulate matter, back half (gr/dscf,lb/dscf, etc.) Ccond = concentration of condensibles (grain/dscf) Ccors. = concentration of coarse particulate (gr/dscf) COir = measured concentration of a calibration gas when introduced in direct calibration mode Cfa = concentration of particulate matter, front half, actual stack flow (gr /acf) CF = concentration of particulate matter, front half (gr/dscf,lb/dscf, etc.) Cgas = Cavg corrected for initial and final system bias checks (Equation 7E-5) Cm = average of initial and final system upscale gas calibration bias checks (ppm, percent) Cma = actual concentration of upscale calibration gas Cmetal = concentration of metals (ppm, Ilg/ft3, etc.) atomic symbol replaces "metal" CO2 = percent carbon dioxide in the stack gas Cp = pitot tube coefficient (0.84) CPM10 = concentration ofPMJO particulate (gr/dscf) Crad = concentration of radionuclides (pCi/dscf) CS = measured concentration of a calibration gas when introduced in system calibration mode Cx = Any species symbol may replace X. Units may be expressed as ppm, lb/dscf, etc. C x (corr) = actual gas concentration corrected to required percent O2 Curies = Measured radionuclides per sample. Units may be pCi or uCi. Dc = jet diameter (cm) D/F = Dioxins and Furans (See laboratory report for D/F descriptions and nomenclacture) ~H = orifice pressure drop (inches H20) ~H@ = orifice pressure (inches H20) ~Hd = orifice pressure head (inches H20) needed for impactor flow rate On = nozzle diameter (inches) ~P = stack flow pressure differential (inches H20) Dpso = 50% effective cutoff diameter of particle (cm) Ds= diameter of the stack (feet) EA = percent excess air ERB = emission rate of back half particulate (lblhr) ERcond = emission rate of condensibles (lb/hr) ERcors = emission rate of coarse particulate (lblhr) ERF = emission rate of front half particulate (lblhr) ERgas = emission rate of a gas (lblhr) ERmmBtu = emission rate permmBtu of fuel ERpM10 = emission rate ofPMJO particulate (lblhr) ERrad = emission rate of radionuclides (pCilhr) ERx = emission rate of compound which replaces X. Units are usually in lblhr. Fo = Dry based fuel factor. Ratio of the gas volume of the products of combustion to the heat content See 40 CFR 60, Appendix A, Method 19, Table 19-2 for fuel factor values. Kc = Cunningham slip correction factor A = mean free path of molecules in gas phase (cm) . MB = mass of particulate in back half (mg) mmBtu = million Btu Meond = mass of condensibles (milligrams) Meors = mass of coarse particulate (milligrams) Nomenclature Md = molecular weight of stack gas, dry basis (Ib/lb-mol) MF = mass of particulate on filter (mg) MFP = mass of particulate matter on filter and probe (mg) mmBtu = million Btu Mp = mass of particulate matter in probe and front wash (mg) MptvllO = mass of PM 10 particulate (milligrams) Ms = molecular weight of stack gas, wet basis (lb/lbmol) Mx= mass of species "X". Units may vary and other descriptive subscripts may apply. ~s = gas viscosity (poise) Mwx = molecular weight of gas species (g/gmol) N = number of jets per plate N2 = percent nitrogen in the stack gas O2 = percent oxygen in the stack gas 'l/6.P = average of the square roots of 6.P (may also be referred to as AS6.P) Pbm = absolute barometric pressure at the dry gas meter (inches Hg) Pbp = absolute barometric pressure at the sample location (inches Hg) PG = stack static pressure (inches H20) Ps = absolute stack pressure (inches Hg) PStd = absolute pressure at standard conditions (29.92 inches Hg.) e = time of test (minutes) Qa = stack gas volumetric flow rate (acfin) Qs = stack gas volumetric flow rate (dscfin) Qse = actual gas flow rate through the cyclone (acfin) Qsee = actual gas flow rate through the impactor (acfin) Qw = wet stack gas std. volumetric flow (fe/min, wscfin) R = gas constant (8.31451 J/gmol-OK) Pp = particle density (1 glcm3) Ps = stack gas density (glcm3) Tm = stack temperature (OF) T s = stack temperature CF) Tstd = absolute temperature at standard conditions (528°R) Tt = Duration of test run in minutes. Also see e Um = mean molecular speed (cm/s) Vm = sample volume (fe) at meter conditions Vmstd = volume standard (dsct), sample volume adjusted to 68°F and 29.92 inches Hg. Vs = velocity of stack gas (fpm) V w = volume water vapor (sct) at 68°F and 29.92 inches Hg. W1wc = weight of the condensed water collected (grams) X c = subscript referring to carbon monoxide, CO . Xd = fraction of dry gas X H = subscriptreferring to hydrogen sulfide, H2S X]\; = subscript referring to oxides of nitrogen, NOx X s = subscript referring to sulfur dioxide, S02 X SA = subscript referring to sulfuric acid mist, H2S04 Y = meter calibration V-factor (dimensionless) \If = dimensionless inertial impaction parameter, 0.14 1 ~ .. J Sample Equations %1 = Vmstd 0 (Ts + 460) 0 1039/ (8 0 Vs 0 Ps 0 Xd 0 0/) A =02/40n s s Bws = Vw / (Vmstd +V w) Cs = Ms 0 0.01543 / Vmstd Ceond = Meond 0 0.01543 / Vmstd Ceors = Meors 0 0.01543 / Vmstd Cfa = Tstd 0 Cfp • Ps 0 Xd / [Pstd 0 (Tm + 460)] Cf = Mfp 00.01543/ Vmstd CPM10 = MpM10 • 0.01543 /Vmstd Crad = CuriesNmstd Cx (act) = (Cx (avg) -Co) 0 Cma / (Cm -Co) Cx (eorr) = Cx (act) • (20.9 -desired %02) / (20.9 -actual %02) 6 Cx (mass) = Mw 0 Cx (ppm) • Pstd / (R 0 Tstd 0 10 ) case Dpso = -J [/-LS 0 \.jf • Non 0 D/ 0 18/ (Ke 0 Pp • Qsee • 4)] PMIO Dpso = 0.15625 0 [(Ts + 460) / (Ms • ps)t.2091 • (/-Ls / Qse)O.7091 ERs= CB 0 Qs • 0.00857 EReond = Ccond 0 Qs • 0.00857 EReors = Ceors • Qs • 0.00857 ERF = Cf • Qs • 0.00857 6 ERg-as = Pstd • Qs 0 Mwx 0 Cx (act) • 60/ (R • Tstd • 10 ) ERx = Qs • Cx (lb/dsef) 0 60 ERmmBtu = Cx 0 Fo. [20.9/(20.9-02)], (Cx in units of Ih/dscf) ERpM10 = CPM10 0 Qs 0 0.00857 ERrad = Crad 0 Qs • 60 Ke = 1 + 2 0 A • 1.257 / Dpso A = /-Ls / (0.499 • Ps 0 U m) Md = CO2 0 0.44 + O2 00.32 + N2 00.28 Ms = (Md 0 Xd) + (18 • Bws) /-Ls = [51.05 + 0.207 • (Ts + 460) + 3.24 .10-5 • (Ts + 460)2 + 0.53147 • %02 -74.143 • Bws] • 10-6 Ps = Pbp + (PG / 13.6) Qa = Vs· As Qs = Qa • Xd • Ps o Tstd / [(Ts + 460) 0 Pstd] Qse = [(Ts + 460) • Pstd / (Tstd 0 Ps)] • [(Vmstd + V w) / 8] Qsee = [(Ts + 460) 0 Pstd / (Tstd 0 Ps)] 0 [(Vmstd + V w) / 8] Qw = Qs / Xd Ps = Ps 0 Ms· 3386.39 0 10-6 / [R· (Ts + 460) / 1.8] U m = 100 0 -J {[R· (Ts +460)/1.8 0 8 0 103] / [n 0 Ms]) Vmstd = Vm 0 Y 0 Tstd 0 (Pbm + ~H / 13.6) / [Pstd 0 (T m + 460)] Vs = 85.49 0 60 • Cp • -J~p 0 ~ [(Ts + 460) / (Ps • Ms)] V we = Wtwe • 0.04715 Xd = 1 -Bws APPENDIXB North Yellow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data Yellow Cake Dryer Baghouse Preliminary Velocity Traverse and Smnpling Point Location Data Particulate Field Data B North Yellow Cake Dryer Scrubber ___ ~}U!:L_ Field Data Sheet Plant: Energy Fuels R{fsources, Blanding, UT a .'J i ..,i-~ '7 Date: 'I" I / /·b i 4 ;4' Time DGM Traverse 1I1------,r-~-:-::-:1 Point II Clock I Min (0) (11') 2 2 3 3 4 4 5 5 6 6 7 7 8 8 Total Average ) :l.;/t) I 0 II j lJ,3o(,:; 15-II ~(),V) .;/(6 '3 D II Yl. 'JSD ~I (;,. II L{ 7.L '<.:{ '6~ I -0 I' r-_'_J_ "_ I' /i'Jj)' Ij I :;'\ • It, 7S-II &\0 .-6~~ C,) Ill} S'bD tL).5-II_Si~'· 1lD I Z J II loD . v&() ~JLJJL' 1.,)'0 J s---o II /2 c\, (;Ot>·! J 0 ~-II 1'1,\0 . 'L.-~) l ~ D II I ... .{ .. ~t-{'l.l"--J,---I \ f ,J' ' r-k~-' 1I15S . \ s-() tL'tL 1t-"'lL'" II ,~ I t<t~ II(~ \.1 IJ • t.P lil1ll~O) ,0 'Jc.;/ II f ,-L '( I,· . '11/ 00 '> J.~{L '1''''/ -1 ~/ . o~5'111. Y)~-' \ .')~ . c-, t S'ILL0i-)<51 V Ib ''-; II l' ')1, (,?,~ u~, L· ( ,')lo It -'~ {0 uo() I' ')G I J') L / V<6 D !-")tt I ('')t6; (l\.C; i .<tJ<-/ I {-0'- OSi: I -(p<1 1 L~ Jl "rjt~~':; ! • "i' "'}--, f,"--( '-f-! J, -.i... .OStLy f·~t L 1\ "-'{"L /o~; , If I { I' \, U ~' -0&5" , ! -1 I I -i./ I · -, !,t~-=~~~\ ~y' ·0V}--I f If' i '1.1., !., !"-' .).-~..-i1 '" - -(;{J c-II ( ,( 7,1 j. r -, I \j Additional (Extra) Leak Check Information DGM before Leak Check Vac ("Hg) '_ ()J:.-1r•·· TETCO _:~/ Filter ~~----.::?l._ Sample Box ___ v Location: North Y cHowcake Dryer Scrubber J Operator: Irl4 / Rate (fe/min) DGM After Leak Check (~ ~' ::tel '1-0 ~\ 'iJ'G <G ?5- ell Vt ---( '15 0> ~ (., {'\ r t-1/ ,"-'-'1 (1D 'i,i) --I , --to '_) }-0;-- <;-s-- 10 7 C;! C( i- lou 101- io3 lOG (1/8' ~~; L: ...... ~ \'./ l, .1\ Ct--}- ~~j-J Ct b Vac ("Hg) Page 7 ~-Run H ! r BO N A Stack Diameter 18" Port Reference _0,0" Ports are 9.5' Upstream from next disturbance Ports are 9,5' Downstream from last disturbance Assumed Moisture 4-13 % 1 ~I ,. Probe L '-j' ~!S) Cp 0.84 Nozzle Calibra"tion " "7 (' I '<_ c.: ( 3' 7. C/ 3' \~ 0 ~ ~ (..) (.l ~ ,",' • (J Avg Dn 3 ftJ 2-,~'nches Gas Bag H'D f Console ":l' . ./" ("'.~ V-Factor -'-, '-J d- t.H@ /.hS' Z.. in H20 Barometric Pressures Pb,,, _ 2~t{, >L.s~=~_ in Hg Pb Z i· '-t r in Hg p---------/p~; () _ [) b in H20 Leak Check: n-'/min vac in Hg Pre O'fl O '}( Z_~ L Pitot Rate -Z. S---' In H20 ()' C) Post f'7<. L (lJ)--<yt. L Water Collected ? ,*] tr f/ g Rate (fe/min) Time Sampled f)>-..v-c min 1"'--',/1 Review K= K ~- @Tm @Tm I C9 J IIi i Field Data Sheet 'I te.r'.dU ".'·-1 . ,'\ ) ,f A' _..,.."TEq'CO \"\ .... _" 1 Sample Box '. " , (~\ ,-/:Q0 I, 'SD f.{~ 5>- {!:I- AH> f ./ -u.~ lr rt.) ~o 4.<> 1- "6' '5~~ ··tG- $., Plant: Energy Fuels\Resol;lrces, Blanding, UT / ,I I Date' i,' ''I I c' fi /:1, / /' • ; ) ;'.e r t .... I Traverse Time I DGM I (it~~O) t..H (in H,o) Vacuum Point Clock Min (0) . (11') Desired Actual (in Jig) 1 i f ',L\-!:, L~ 0 J <;"(;. ! I j ·ol~" ( .·~D {. St.) ·S 1 '[;5'5/ { ';'1!. ~'1 ':t t{ -()":j-::7 [,,) 0 I·'~lj (~ 2 1'~·\) 2. { O· S ~ L:~I "oS 0 { ,'4y,' l'-~S .... 1" .... ~. 2 'U'tiS '?Ll·D~·i.;·· .VtO~ 1·4 -.\-.. . "} ' ,~ "'\ i ., ',-rr; 3 ~ ()I.--' 1.~)'~:(\ . O';)D I'se, \. s'l; f~ I,:;. 3 ~ ( s: L -t<;"· S'L{ {"J .(/\ ~-J ·(;d l·iJ ,~ J' t;) 4 '~.~ (5 '7 C; ;1-. 'JI> t ..... .' ",1) j Irx~\ t. U·.I IJ-) /. 'r"} :~J:.' 'l.,Y. C;" l;}." /J .. ' -u (> ),CJO ,! /" ( 4 'V' I...·/·i{ I. '-"{() 5 'j~ (> 0' \' I''''' '7;Y. .). {~1 _U(; /'(10 i . Gj{) ....... ~,.-. ((, ',1':;' 1..-~L;' i.d) V • 10(;) /. S-'C !. <; L, ,..- 5 ct~? 6 ·S£/) () /1) CI'1. UtS' . ((/-,;" (.~·L }·fZ i>1 r 6 l{ 0 S' "-I) ",' .,.j 11 Ii {'ClD 1 '" .' ,c1 )' ,(,'V7}' • \ v-i· L,t () L. /) l.r, 7 4I~ 11 )Li . 1 tt't .Ot1 r l' l.!iY 1,. i 1'(:) ! ' \ a \_j i 7 L(~~ -; L\'~~' d \ S-' \ '\' -{O r: 1'"+-' i·' t ':}-') 10 8 ~S0 ') t.-·;:1 j~ ~ [) .. e11~' of. [., Z { .(;: 7.~ J f.,j ~~S" 1) i"L .t(f1~' -(J1(-! ·{,tL ( l l f 8 t 'b 1- /~J t~~:qi Lt~0 3/?L/,(:/! ~. ;'1 . /..s;·y> / Total . .-1 ' 1 /;1 ",,' .' "j.L vl t.; i/-' / '2., .. -({ . I tJ! ~ (..1 .u -l., i y:/ {,{;' i ";. /" j \ L 1 \ ~J • .-__ v __ _ , (':\ eri.L " , C' '{', tv' I 0:0 ,\ ',) " . ' ___" • I,' v I; Average Additional (Extra) Leak Check Information Location: North Yel~owcake Dryer Scrubber Operator: \/ ...... ' , ) I Stack (TJ l (L, II C, 1/ C;'" r F1 \ I t::" 1,1-. ') 1\ L) t l '-1 1 r::r ~ l ) 1.-<~1 tL~' 1\ l,\, It [) I'Ll l Z. \ f Z/{ Temperatures (I) II DGM Temp (Till) Effluent i l><5 I d~_ i.·~ -v I.£.'()I ...... / -~:S~ ~I '~.J ': ... 7 3 j '/ ~ I I S-<;r '1JA:71 I e;--.t:; I '.-~ . "'l.Lt{) I s-: . "';,01 '1/ t.;.~I· I .r}.Ll-tl I .;,:;-~. II i:) L I '/ r (..1 -~ .... • ... (i. '-'"' "-'* til I l..; ! J r) ~"" .. ~ !:..) ~ t.,; )'L~ ~ftt3:/~\~/ 1 5-' \ II (itLLl2J I 1..,:; J) 1 i .. rS 1~:·lT3f 5-=-rlll 0 o-r7 0 -} IS' \ I 2>\'$1 2~.1:~ls2-,,11 /oZt / L/) t5'~~FU-f (l'{ 11""qCl·-~>~.-IIID(:17 t>~1' L~?rlZTr I iLf?r'~"3 III {j:> I I D L:; -"!til 5'1 i;)</7 I '-;~S-L?I 5'-( II! 05 I [ D ~j 7 r", I ;l-ll; /7 ('11 ! 2 II '/1 <.: ,/71,j " '" L, (,,".> II 1/)_-" 1 D '1 ! D 7 ')[plJ\/ -. [ I" ( I,.f I v\"'A, I " \" \ /1 .--.f ,:'//.S·'t DGM before Leak Check Vac (ttHg) Rate (fe/min) DGM After Leak Check Vac ("Hg) Page 2J of Z Run # r BO N A 18"__ Port Reference _0,0"_ ~ Upstream from next disturbance Assumed Moisture 4-13 % ---- Probe ZIt) Cp 0.84 Nozzle Calibration 7.. <> I -(, { -( -:'/ C-; ""t c" ~. SO _,_",_T_ • .)(5 C'l Avg On. '~ «"6;: \nches Gas Bag (j -( 0 'j Console -:':J Y-Factor-(;7 ~ b L\H@ I' (P 1>' Lin H20 Barometric Pressures Pbm 2 '--(. sj-' in Hg in Hg in H20 Leak Check: nJ/min PI tot Rate InH10 Rate (felmin) l l '-{ . '-I., $ p)n ___ _ 'P li ,' .-" C: ' LJ ,b P..ne iJ . D D ;1-J 'l, Z. ·l C;- (),U Review K= K =, Post _ C~" I\'j .... L)u .. \ .,-;:-=:-. I .~::> . <',~;,;> C;:-C.J .. -~ (,-:-. C-,(' g @Tm @Tm t " ()~ '~ il.,.! 30 ~.s s 2.·.M~ ~~, 'Sa L15 .~". 00 Co I .~ :<0 \.It;.., Ii,. Co ~ Field Data Sheet Plant: Energy Fuels Resources, Blanding, UT Date: t"\ /;z.l:a / ~ ") ":'1..1.<:\ DGM ,1p TETCO Filter (., \')::,/1 Sample Box f\ ~-'---- Location: North Y~lIowcake Dryer Scrubber Operator: ,\(~.,,;,m r.,. Point Traverse II Time, I' Clock I Min (0) (n') (;1111,0) Desired In 2 2 3 3 4 4 5 5 6 6 7 7 8 8 Total Average '"'l! .~1 ~ ~ ,,;;-~'j o ~ ..... n ' ~ ~3 ':\(~: U7.:, bO '''It:'':, q(,,; \rl~~ ~ ~ "'" \' -'.\'" (, -~~:, t ~)t! \\l~::'~ \,?',Ci :~~i ~:)."' t r~ ':?~7>S,'Ct \1.0'60 ':; ~ L, . ~ \fl·11 . (')? 0 YO"'iJ) I, 6'7511 . e~~,O ~ { ., ? ..; ''} ~II . ~ ~ () iJj '2. t'tJ " :;:. ~ (:11 ~ rl, '?j 'f li~} 5~)~; II • (\~ ~;, ~~~,; . y ~ :;~ II , ~ ("t;,; i~ l", »--1 ~ r.~ ~\:~II. \ n:-:', ~7~.~~oll~, 'i~. '1, • '1~ ~ \:~" p '~~-J ,::"j 'f) "'1.. " ~ S; ("',II,,,,, ft", ''1 :~:., 1.~~13: 't ~'~~~ (, '2,,' \:~~. ~,\ :(:;. 2. 2 .?;'? I \1, '.:\?, II 1 ... u ,,'3,3 11,,?, .:. JL2 a ~~JtL~" :i ~ t;:,,~ I ~ ~,e;~ IL 'ii, I it ...,~-' \\ ~ T\ ~.)'I ~ ~ --j~) I ~ II ~~~~ ~~i .. "-:110, I \~ _ ~'l :-:.~ jj , ~ n-~[;c~ I ~ f\~--)~~~; i~i l \\ Q~'~." :i,~':'{!11 S' ~ ~~':~:1 r "'-.~ ~ 1\ l\...., ~+.":t 6 ~:):: ~, h ':;-;:' ~~II " l';/"n,i" II \.. (,,-:; 5 ;. I) ;~\I::) (;~~;' S:::.!.n, ~n,;:-·II. c,(,i:" 1 II '" ~~ \'~ p_~ c~ e;-:: ~)-~j'~" ~ r\t?=-II'_D'1'·..'.II~ l~,,: ), ~~:~.l ~> ~,~ '~":)" (~:11 ~ «c; '?-,5J\ 1,1 ~ "t h \1 ~ ~ (~-1" f.:;) ~ o~~~, i!oq ~ r~ -~) t \~, ~:~ u5_ !1 t\\ n ~ ~ ~ 11L~ \ :?~- ~'~ \ u 't :2 .. ~ ~() It\ ).2 S II 'Sf.,.., ~~ (1 :~, :~II • (\t{\, t:,.11 I!. n I ;) n q :~, 11";f" II ~ 'il C"'j H~,}"l~ 1'2.l~C II ~:::~--;i , 2~{~ ~~ ri: e,i " t.~~) "::-:-t~ ...J __ _ './ Additional (Extra) Leak Check Information DC;M before Leak Check Vac (tlHg)' Rate (fe/min) :~~r. ~~ ::-~~ A ~> , (i ~ (::) (p" () ~!:~7 6 I 2. ~,;l S I }.l,..:",; ';Uo~ I 2~10 17:=:0, -:~.c.,:,· I?:'; <:) I ~} "} n LiL"i/.a 12-; 3. 1 :t~l :~~ "j ,'-](i, I''Y. ~~7! 61 :?:'? (:; ~:rJ'-; "I, --o"~,1,", I ~,), ',"7 :,1 _~~_ -'-~ ii ~-_" ____ ~-u .. _ li 1 ~~~J ~'1 I LJ I ~2~:;.J.-7 I:) ~1 c:. ~)_\L-. 'l I 2# b~ I L1 2 t;::,l?l I 2~ ?:<<, I :.:};.;~:.) ~) J:~~~lS '25l t 12.~ ~ 12,( .... it 1~:;~ ~(} 12(~~ '~ '~9C'C 10J I: c; ,-"',i .-., sf:_~ tt '.:' • -.. ...~...J:>,. \'") ~ #<'..:-,).*~ :\ I""i cl (:, .e.-40~._._..,_,!! <0;,)1 5:;:, ~:~ e,-l .. ,... ~'~ ... S~~ ~;':') s'Y ~:~ ~~J r~-" :~,,!!:.? ~~~-J 5:~(~ ~~6 t:;~. :! ~ I) ~ <;2,. {:. -:r: ~ ;~ ...... ' ~:~ i~4 lac:. '/1 i ~l ~'J ~"r') <1 \t t~ i~ i , C'~,o °l'S (1 :'> ('1 fr OF c;,-:? ('1 \\ (~] ~ t.,~ "1U (\ .~ ?'i..:' ... 59:l' 9; 8-J ~{.; q-; ~6:i ,: f;, "'~'., 'it () .(~~.~ teL t tJ{~ (n 9" 0' t \~': ~o~ Z Yh 12.i .. 1\ 17,)(7 ~ I ,f,-) .. II q'~J 1 \~()~::r.~ DGM After Leak Check Vac (tlHg) :) " SOl() ~ :3 Pagc~~ot~ Runll }_ I BQ N A Stack Diameter 18"__ Port Reference _0.0"_ Ports arc ~ Upstream from next disturbance Ports are 9.5' Downstream from last disturbance Assumed Moisture 4-13 % Probe 2?-1 (; Cp_ 0.84 Nozzle Calibration ~ :~'f,( ~ '3 -:' (1 • -7) ~, (l Avg Dn:~?'C<? :) inches Gas Bag H -n-'; Console _·' ... C __ _ Y -Factor "t-:" t) 1(, 6H@ ~. ;..,9.:1 in H20 Barometric Pressures Leak Check Phlll '2 I; , <C, c} PhI' .2 t"~ _ q ';.. Pu (~. 0:: .'~ Pre f\,l/min (,). \') <::> b vac in I\g ~';',}. Pitot Rate 0', <':' In H20 • '},:'~' in Hg in Hg in H20 Post ~}(-,~~ t :?:¥ '?(,F-. f" --) _ Water Collected g Time Sampled .. min Review K= @Tm K= @Tm Rate (fe/min) ty i (0;(1 :~-" L! 1.. .. C :l L5 .~() I,S ~ :J 30 l~ ~:. lo . ! (~, r. ;5 ~'S {l II r:', ~, :5 '.') () l!~" . ~] il. G /r {f-( Field Data Sheet Plant: Energy Fuels Resources, Blanding, UT Date: I:~ ;":,.":'1 ,< TETCO I' Filter i¥, \':lli G Sample Box t\_' __ Location: North Yellowcake Dryer Scrubber Operator: ",,,~ \~~'. fC' C ~~ '"'--p, Traverse II Time I' Clock I Min (0) DGM GP t.H (in HP) II Vacuum II-----r-~:...-__.=----_,_--__,--:....-_II_--_r-"-...:.....::.:.:- Point 2 2 3 3 4 4 5 5 6 6 7 7 8 8 ;rota I Average t'~·, ?'~-l 12.3): 0 _~:) ~~~3~·· ~ L:;l:;~' J.-~!() :?~ .. ~ f:; .~(';,(., ~ ~~~: ~-;)~'?J () ~;\:;'S ~.~\).~--,,\) :!-;-'-j ~~) ?>Jf.'f,>:-:) l~ ct.:., i~:?,O l~ .~~ ::~. ~~S.\\ ''-~~~ ~~-~ I;; ('), ~ iI ~('. (11") (ill 11,0) Desired I Actual ~>"r) .• '~I"'O II • (,'t. ~j~ II \; . ~C') I ~. ~ C"') Sl(1,lf. :::' 7/\ ::h l.?! () l.,~) <n .:!!'!LCJ.O I 'l 1", 'lL ;'0' n --.LL...L"'JIl:, {::; 2.!\ 2hS • ()"A~< ~1<1; ('; Li ~}1() ..£,'"'t (" • r/'11') . t~ \." ~ -I' _ ~ ~ :~w i ~ ~~f 1~ r. #:-1"'; I-~ ~.) ~. '~ ~ ~,,1~ bLl (y ~ 'T?,,() IIJ. li II U r,-1 r, Lb:}'~~" ::; II " ~ II 'u " -; 'i'i t.::: -.. "'''II Ii f'" II I! ,;:; ',,;' ",XL ~ ").,j ~ ~ (1JJli-"-.L ~'n°-y (il ~ C~~ t ~ r}~l) .=~:I !I i"=1..... ~~ '.~: . "C L __ L4I., ,:I .. ''1 ".'<.0' \'2l!l.,. (t "~ 5 fl?-.i,() .k ~:) :i, ~71f '3 , 1;~ ~ ) ! 5 ::'), :(';(l tt't,) ) )'15' z ~ ( ~\''J~ 'i:-e:~' • ,,, .... : ..... ":, •. "0: ":: " h i"'"I;:J n n .~ of ()t1:~ • n~ ::- ... r;~r.t: f'.j J t:,"'; c; :~ n ;9~"?~~ " " ; (~i~ I~ tl ~ or, : ,,('\~~ : ~ ~ ~. • :; 1':, ,~ ;\ :--',~- .. t~(./(I \I_~ ~:~ 4 I; t. e:)i~ f~ ).~ ~ :~.t ' .. \~"7~~t~ ~ t,"-lj ?~\ ,,' '} ~J\ \-4-~~1' L:i~y • f.t)~~> U~C1l~~ ; • '"11iJ l t\ ~~-,.l.~ ~ r, \,':1 g: cc ~ ~ -1' 't ? t-... 'l:. J .. ., -'c ' (ill IIg) ~ l\:, '. 0: • .....::... '--'-..t." ~~1 ;~ .~ --~~~ -;;.~ l t d.~. n '~(~j ~ q ;05, u !: r,'2, t; ~ ~~ f,j '?li ~~~ : (;:::, 4 " ~ () :~~;, c, :\ (B"} :~1 ~ c:)--~ :~ .. :, ..1 C' ,~:;) ':i] (';, e..:., \~. C ">: I;)) ~ ~ j.O) ';>~; ~ ___ ...:.....:~ __ ,"</ '~ .. ':0~ ,.,/ 'r~ ... T --J' -::' t~~.~., ~ .,." • J ~,,_ : y 1'),': J"':': , ~.,~'tn ~ i!-... " ,. c ';".1,. !' (-. Additional (Extra) Leak Check Information DGM before Leak Check Vac ("Hg) Rate (fe/min) ""r-?-t.;., 12.('>;(') 2,c) 0. C .. (j, :C:l ~ I) ... ~ :;~ 12. 'H ). ~ \<) 2~'~'D I-L ~ q 1 L.tf, tf ,,~' :-, I'fj, I 2. f::',C} 1 } ~ r:l'i' ~:,\"? ::'.~.~(~ I 2_ t;=jf! 1 )'~ :")(') t~~ r 1':"#.'1: ~ 0 __ , ")) c~ I <:l, I ", L.,\ q ..... ~ ....,~" ,~ b ... :". T, ,. or: ,. .... '1 2:5}' 1)--::.Ll 12 ::7 i~ 1* r" -::'.'-;19-. 1 ;:'"::,C,, 12~'~ c' yt lr I).~fj' I"') !.t"") t~~)?_p !' H t!. I I'" r-e~ ',~' J ~",.'>~:;; I '2,Y J 1-2.:;<';t. 125:: ~~ C"') .... ~ <'--- '.:'.~: (, I·.~~t~''} 17 .. 4 I ''';'~ t.f I-:n.p,; .r..... \t i, .. ..... l~ t' I ~" g ", I ' , ... l '*' -1 .. ~:~ ~'\ ~)?~ 2, ::.c 1 )"~i S 17 ,~~ :::, ~~~:~ ... f'7 2:~t~ t1 .-:;~ l: C,.~. ~~ DGM After Leak Check 92, '1~ (' ';, \l ..... " ~~l ~.~ ~1 () Cl Cl q • Ct. -;~~ (~ t..i . , ~s Qr, I)''''''' t:~~j y (\ U " t:./, . ~ (: N.k In ()jl .''-) .. ... -~'" ~:::J ~ l':) t1 ~.~;! q'-" Cr: ; C) S ') ?" qr:, ~o t ~ o'·2.-p ~o i~ ~f':~b ~ (;rr, ; ('.:-':1 \ \ t . i,,":\, t:.~ ~? .. ~~"'J ' i ~.~ t~ t. ~'; Vac ("Hg) " f) Pag~ :'. of~ Run #-.-L.- r o N B A Stack Diameter 18"__ Port Reference _0.0"_ Ports are ~ Upstream from next disturbance Ports are 9.5' Downstream from last disturbance Assumed Moisture 4-13 % Probe '2,,:"~ (.". Cp _ 0.84 Nozzle Calibration ~ ~:')~, ~ ~ ~:) ~, L " ?:~ (t • 7}~ c' Avg On ':)?()::',~" inches \\1 .;;:. __ -, Gas Bag,;"\ " r, i Console ___ _ Y -Factor "(1 ~ b t.H@ ;~ ,J r.~ if, :'i, in H20 Barometric Pressures Pbltl:~ ~ " S :~) in Hg Leak Check: Pb" ), \1 ' L~ .t:. P(i f:, ("; (,., Pre nJ/min ('; ~ (,(,,If' vac in J!g .... ~ :~'I , Pitot Rate (). () in Hg in H20 Post (':',,"'1..(',-;r., ,\ (), ;,""',;.:,. () In HlO • :'. ~':, ~ .;) ,:-~I ",; ( (p f (0 Water Collected g Time Sampled ~'1; {) min Review A K= K= @TIll @Tm Rate (fe/min) Yellow Cake Dryer Baghouse TETCO ) 711 L-! Field Data Sheet Filter ,(J C'le.:· Sample Box---iZ Page _,_" _of __ I_' I Run 11 __ /_ Plant: Energy Fuels Resources, Blanding, UT Date: (;/ -./. f: --/1 Traverse Time DOM !1P !1H (in HP) Vacuum Point Clock Min (8) (fI') (in 11,0) Desired Actual (in liS) 1 (ell J 0 1 C;,J.1J .,/] ;;.. 0{3 2 .... £:'(; / 2 j t;: i c~fJ ( ~(t[; ,J-).-jf 1.JL '/(9;-'6 3 ]~ 0 j 11, (.1 Ie' J{) J( f;; 7 'f 97 {, 4 .} C-'7 12. C I J. ))~. . (p 7 J..J-I j.J"j 7 5 (fC' /J(;,C(7J 7 ") I C ).. b)" lit). y';-? 6 ./ L·~' I<--Ie, ~?) ,G 7 )~17 )'~-1 7 1 I/·'{(j -' b C>' IJ~l( Ir)... ,"Ill J' i7 () II tt) J- 2 7'"'' _. c-/6j'----1 t) {/ ,ye (e g L> I, ?() .I 3 '9{~} 17C11 (r; C L{ £ Ie 6(;) /< 60 ,j---- 4 C(C I/e,/. L-/ (F) /(,(tf Ie f;:) /t 9.~ .,)/ 5 It/C) / 9 ~ ) lr~) hh' ).)/ '2J)~ ( 6 (f{' JO) 7/.)' ,&1 /..,).9 1-1, (1 it' fl.,'tl r 171" -)~ ! 2, ,) -tj- Total .' / '7. ) (' U ~1.' ,/;; ! I /; y I 7 .J, • (~!.. /,L ,AJ--:';'y Average .J I ') I)? ,'----,:-.,-I. ") Comments: Time Baghouse !1P Time Baghouse !1P [t/':c-!{) (,.f I 7--~. 12·'(../C) ,-' I 1/ : [/t) L{ J-Il;)~,1 .;-: CC' /J..JJ) II () / )-:'f() c,( () I/-'~( () &/, ( Location: North Yellowcake Dryer Baghouse Operator: / /: II, f C' /, r,~ J p ; Temperatures ("F) DGM Temp (Tn» r B AQ N Stack (T,) Probe Probe Out Filter Effluent Out In It! r'-J.7{ 2/:; / .. ,Jrc; t/ t·, 7] 7,/ / ()f~~ :2.'») l' J t1t:" '-( J. jc; 7~;,}! Stack Diameter 16"___ Port Reference _0.0"_ I v" b ?Jf-),{;&/ ),,"1 t:/ t-(C 77 9'6 Ports are ~ Upstream from next disturbance 1/t:J J-;J~7 )--; ! 'J-.J.J"-(1/3 g)-. 9";2, Ports are 468" Downstream from last disturbance Ift1 l,.{t(j /]7 )I-~;' i9 ty--L.// ftc? Assumed Moisture % / I (..'l J.totj }~'}r;' 7·) Y ,J-u 83 Yf I!() :)--{ ).. ;-v9 //---0 ~~/ 'Ie fe., {i/p'? Probe I If-b ----Cp 0.84 Nozzle Calihration / 1(:' ).;;0 ),-L(c1 ;II:' [( C; f)-, let! ;z.rL .,J. f'/ ( J;./), , .L,,5 7-.. 11/:) I}-F)) )-7t/ JAil [;16~ 97 / /-" ,-?, ,[ / Avg Dn ,)-/ 1.J' i~ches Gas Bag Ambient Air III J-.)9 7Jt/ 1--11/ U;7 ctt! / ;;;/ 1// }/7r;-)~) b J~'f J. t( !Q if j--Ie J ) I ( ). 7 (~-' ).)~<j 7fi. c-I 'f~ 7{' 'I ;'A r / i L' ! )c;" 9 [ )-/7 r ! {,~< 51, / f/ :: Ii·. !J f.r /';#//;" /Y t." v, ...... .:. :; --IJyl Console '} V-Factor /,(::. /."'6 AH@ l (,/ty/ in H20 l3arometric Pressures , 1,~-~/t-I Pbm -;r,j Pb ,.{ 1, 1/6' I'-=--~-----'--- Po---=:::'" (.; 7 in Hg )-d! .)S inHg in H20 Leak Check: Pre Post I,"/I,/hc-J ft'/min 1 (~t-::' '7 ' t7'C:;~ / i C-~~ (, vac in IIg ).(! D' Pitot Rute 0. (..) (_'~ c' B,(. ~ In H~O t:;:··o ).). )-Water Collected L -' ,/ • Time Sampled / ). r...: i Review hi K= K= IJ.:C(J @Tm @Tm g min North Yellow Cake Scrubber Sample Recovery Gas Analysis Data (ORSA T) Yellow Cake Dryer Baghouse Sample Recovery Gas Analysis Data (Ambient) Chain of Custody Lab Analysis APPENDIXC c North Yellow Cake Dryer Scrubber METHOD 5 Facilitv: 1. !./ ; / '!i .; ",./. r: .. ' / i.,: - . ..,.. Date: ------------~---Stack Identification: IMPINGERS Run: ----Sample Box: 4-----:;/~, -- lmpinger Number 2 I 2. I 4 I 2-,1 6 Initial Volume of liquid (H20) in impingers, (ml) drop out I 100 I 100 I Silica Gel Total (g) ,7 '; (:--..-. ...,/ ================= IMPI~GERS Sample Box: ____ _ lmpinger Number 2 3 I 4 I ~ 6 Initial Volume of liquid (H20) in impingers, (ml) drop out I 100 I 100 I Silica Gel FI'nal (0) ~ (' (, i C ./ <-, v (,(7.,-)'0 . ~, I /' ';' . L I / >f.jv '-"f In iti al (g) .:;........~~.:...-..,..~~~~-+---::~--:----l-~~--+--.."...,r--,.--'--+-...-::...---:---:-:--~. I!VIPINGERS IMPINGERS Net (g) ======~==============================~======= /'''"-..:-'''' ·'7 ./ Total (g) vi' ================= Run: ----Sample Box: ____ _ lmplnger Number 2 3 I 4 I ~ Initial Volume of liquid (1-120) in impingers, (ml) Final (g) _______ 1-____ -+ ____ ---1 ______ +-_____ -+-___ _ Initial (g) ------1------+------1-----+------+------ Net (g) ======~======~====~======~====~====== Total (g) ================= . --_. __ ... _-_ .... Run: ----Sample Box: ____ _ lmpinger Number 2 I 3 I 4 I ~ Initial Volume of liquid (H20) in impingers, (ml) drop out I 100 I 100 I Silica Gel Final (g) -------+-------+------f-------+-----+------- Initial (g) -------1------+-----1-----+-----+------ Net (g) ====='===========::!:::=:============= Total (g) ======== Plant Analytical Method ___ -----=CO-'L-;,u:,.-!,-",' y~' ~r-_' ____ _ Date r~d-/) Test No. / Gas Bag No. ;;1-[ 7 " Ambient Temp ZJ., Operator P//h I I Date [1/1 -'i A / { -;? --'-t'~tr~'--'-'I ,"-'_'-""' Test No. _--,.~r~-}/-/....,..,.....::; Gas Bag No. __ i-:-t_---:::-(./_" _{' Ambient Temp __ '-,~-+\_L __ Operator __ +t4",,",i~,-_~-,\,,\ _ Date ----,---Test No. ____ _ Gas Bag No. ____ _ Ambient Temp ____ _ Operator ____ _ Gas CO2 Gas O2 (Net is Actual O2 Reading Minus Actual CO2 Gas O2 (Net is Actual O2 Reading Minus Actual CO2 Reading). N2 (Net is 100 Minus Actual O2 Reading). Actual Read ;?, 6 Actual Reading :'iet /2,G Net Readin /-.. b I'? f:; Actual Reading t O2 was determined using a gas analyzer A, G /;·2- Net CO is not measured, as it has the same molecular weight as N2 .--/-.b li8 Actual Reading :'let ;L . b ///).. Net Average :\et Volume ;2_ ? /,7, ).._ Average Net Volume -'1 . / t Average Net Net Volume Yellow Cake Dryer Baghouse Method 5 Facil ity: __ ;:_~;.......;..,;......;........;-~, ~ __ .:..-/,o;;...J _-:/_,--,-,-: _,_' '_' {'_/_' <_/~'_' __ _ Date: ,/ ,', './ ----------~---- Stack Identification: \jejll<:,w (0,1<<:, »)c.. q\"'o...:$(/ t J IMPINGERS Run: ------Sample Box: p-, ----'------ Filter Number: implnger Number 2 I 3 I 4 I 5 6 Initial Volume of liquid (H20) in impingers, (ml) 100 100 I I Sih;'ah:! I Final (g) ./ -'" 6 ;:: ::.j, 1(> 7 ", /,;. (," ';'. -0,1 ./ Initial (g) ~!(P. 0 L1'QZ..O (Yc·5-. I 7"'lj! r ...;'I-...J Net (g) --/ull 0 /1., C Lj, / ;L.';;-~t7 Total (g) J.,;, )~ ./ ============= IMPINGERS Run: Sample Box: ---------------- Filter Number: Implnger Number 2 I 3 I 4 I 5 6 Initial Volume ofliquid (H20) in impingers. (ml) 100 100 I I Silica (it! I Final (g) -------+-------~-------+------_;--------r_------ Initial (g) -------+-------~-------+------~--------r_------Net (g) ============================== Total (g) ======== IMPINGERS Run: Sample Box: --------- Filter Number: implnger Number 2 I 3 I 4 I 5 6 Initial Volume of liquid (H20) in impingers. (m1) 100 JOO I I SiLeaCe! I Final (g) -------+-------~-------+------~--------+--------Initial (g) -------+-------~-------+------~--------+--------Net (g) =============================== Total (g) ======== : ~ '., • ': .~. 'i: .. , " : 1,'J '::'.; t' r Chain of Custody Record TAL-4124 (1007' Client Tetco -_ •••• ···_····~··.· •• _ •• , .. • •• • .. M ....... _ •• _ ..................... _ Address. 391 East 620 South .... ... ............. . .. Cio/ •... ....... ... . ..... .... ....... . ..... . ............................... ··Jstate l(ffJCQde • American Fork Ut . 84003 Proiect Name and Location {State} Denison Mine 20111st Quarter Contract/Purchase Order/Quote No. ............... _._ ..... ---... .... Sampfe 1.0. No. and Description Date (Containers for each sampfe may be combined on one fine) R1 Baghouse filter (6038) and beaker 10/?8/12 ... R1 NYC filters (6037) and beaker 10/28/12 R2 NYC filters (6039,6040) and beaker : 10/29/12 .... ... ......... • ·1··········· ....... . , ...... ... . ..... ..... .......... . :: •.................................. ............ .... .... ....................................... 1·. • .................................. ...... ...... ....... ....................... .......... ..................... I • I ••••••• J ......... _. __ ~ ••••• __ ............ _ ••• __ Possible Hazard IdentificaNon o Non-Hazard o Flammable o Skin Irritwlt o Poison!] Turn Around Time Required Temperature on Receipt __ _ TestAmerica Drinking Water?. Yes 0 No 0 THE LEADER IN ENVIRONMENTAL TESTING • Proiect lvianaqer Date Cl1ail7 .01 CuslfJdv.Number , Dean Kitchen 10/01/2012 I Telephone NumbGr iArea Code)/Fax Number Lab Number / I .. ............ : 801-492~91Q6 ... Page of~ site contact I Lab Contact Anafysis (Attach list if Scott Christensen, Garren Palmer mora space Is needed) ... I Car/ierJWayb/1f Number Special Instructlons/ Containers & Conditions of Rece;pt Matrix 0 i Preservatives d \D .-t 'lii. ~ N N >-1 ..,. N -b " ~ ~ ~ ~~ z· , n, III Sl I :r: Time ~ ~ ~ ::l H 0:: !l .:' (~ I ~ ~ r!:l~ <>: "'( --=--t-·-.. • .... 11:00 X ! X ; ,' ............... ..... ........... .. ......... ".~ ...... -.. 118:00 ..• X X !L .......... 8:00 : X X . ... ..... ...... .. .. . .. . .. . ................... . .. _ ........ ........... . _ ............... ....... '" r·······~ ;--........ - I '---'" ........... .~ ............. ". -- .. _..... ~--.,_.,-I Sample Disposal fA fee may be assessed if semp(es are ret8med o Unknown 0 Return To Client ~ Disposal By Lab o Archive For _~_ Months longer than 1 month) ac, Rcquirements (Specify) ~._.~::.~ur:.;'S.~/\;\~D~48~H~o:u:rs~~O~7~D:a~y:'S-~D=-:.:1Lf::... :Da~y:'S~~D=-2~·~1 D:a~y::s_~D;;! ~Ot:h~e:.:r .=a=s= .. D~e=r~m~et=h=o=d=~k_-::::-.....-:~,-;:::---------------------......",,_-___ -=,__--- 1. Relinquished. 'Y .. / Date. 0 \ I i Time 1. Received By , Date I Time 2. Re/",,~~!,;I ( /.~ ---~ol:L"'1f~ r;me.---+12;;-.-;::R;::ece-:::-;Iv.-::e:::d;-;;B:;:-:y:-----------'-----------:-...L..:.~----.t..",.,----- 3. Relinquished By Comments When Complete Email to:DeanorPaultetco@tetco-ut.com jjiSTRIBUTION: WHITE -Returned to Client wilh Report; CANARY -Stays with the Sample; PINK ~ Field Copy Analytical Data Package Prepared For Denison Mines (USA) Corp. Denison Mine 2012 3rd Quarter Radiochemical Analysis By TestAmerica 2800 G. W. Way, Richland Wa, 99354, (509)-375-3131. Assigned Laboratory Code: Data Package Contains 15 Pages Report No.: 53660 Results in this report relate only to the sample(s) analyzed. SDG No. 45792 Order No. Client Sample ID (List Order) Lot-Sa No. \Vork Order Report DB ID Batch No. TestAmerica rptSTLRchTitle v3.73 TestAmerica Laboratories, Inc. R1 Baghouse J2J040470-1 Filter(6038)/Bkr R1 NYC Filters (6037) I J2J040470-2 Beaker R2 NYC Filters J2J040470-3 (6039,6040)/Bkr MWTWE1AA 9MWTWE10 2283081 MWTWJ3AA 9MWTWJ30 2306033 MWTWK1AA 9MWTWK10 2283081 .. rica THE LEADER' N ENViRONMENTAL TESTING Certificate of Analysis November 8, 2012 Denison Mines (USA) Corp 1050 17th Street, Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab Project Name Sample Type SDG Number I. Introduction October 4, 2012 Denison Mine 2012 3rd Quarter Three (3) Stack Filter Samples 45792 CASE NARRATIVE On October 4, 2012, three stack filter samples were received at TestAmerica's Richland laboratory for radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification numbers as described on the cover page of the Analytical Data Package report form. The samples were assigned to Lot Numbers 121040470. II. Sample Receipt The samples were received in good condition and no anomalies were noted during check-in. The sample date was incorrect on the chain-of-custody. The client was contacted and provide the correct date of September 28,2012. III. Analytical Results/Methodology The analytical results for this report are presented by laboratory sample ID. Each set of data includes sample identification information; analytical results and the appropriate associated statistical uncertainties. The analysis requested was: Alpha Spectroscopy Uranium-234, -235, -238 by method RL-ALP-004 TestAmerica Laboratories, Inc. 2 1 I ) Denison Mines (USA) Corp November 8, 2012 IV. Quality Control The analytical result for each analysis performed includes a minimum of one laboratory control sample (LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments" section. v. Comments Alpha Spectroscopy Uranium-234, 235, 238 Sample Rl NYC Filters (6039,6040) and Beaker has an elevated FWHM due to the activity in the sample. The sample was re-analyzed but still shows some slight smearing in the spectra for U-234 but the results are acceptable. -The batch LCS recovery yield for U-234 was initially just below acceptance. The LCS was recounted and is now within acceptance criteria. The achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to historical process knowledge. The sample activity exceeds the MDA and detection limit for all samples. The batch blank activity also exceeds detection limit; however, the blank results are significantly lower than sample results. Data is accepted. Except as noted, the LCS, batch blank, sample and sample duplicate results are within acceptance limits. I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically and for completeness, for other than the conditions detailed above. The Laboratory Manager or a designee, as verified by the following signature has authorized release of the data contained in this hard copy data package. Reviewed and approved: Erika Jordan (~n)!\n~ 2012.11.08 -7'-11 :24:04 -08'00' Erika Jordan Customer Service Manager TestAmerica Laboratories, Inc. 3 Drinking Water Method Cross References DRINKING WATER ASTM METHOD CROSS REFERENCES Referenced Method lsotope(s) TestAmerica Richland's SOP N EPA 901.1 Cs-134,1-131 RL-GAM-001 EPA 900.0 Alpha & Beta RL-GPC-001 EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002 EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002 EPA 903.1 Ra-226 RL-RA-001 EPA 904.0 Ra-228 RL-RA-001 EPA 905.0 Sr-89/90 ' RL-GPC-003 ASTM 05174 Uranium RL-KPA-003 EPA 906.0 Tritium RL-LSC-005 , , Results in this report relate only to the sample(s) analyzed. Uncertainty Estimation TestAmerica Richland has adopted the internationally accepted approach to estimating uncertainties described in "N I ST Technical Note 1297, 1994 Edition". The approach, "Law of Propagation of Errors", involves the identification of all variables in an analytical method which are used to derive a result. These variables are related to the analytical result (R) by some functional relationship, R = constants * t{x.y,z, ... ). The components (x,y,z) are evaluated to determine their contribution to the overall method uncertainty. The individual component uncertainties (Ui) are then combined using a statistical model that provides the most probable overall uncertainty value. All component uncertainties are categorized as type A, evaluated by statistical methods, or type S, evaluated by other means. Uncertainties not included in the components, such as sample homogeneity, are combined with the component uncertainty as the square root of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result is the combined uncertainty (ue) multiplied by the coverage factor (1,2, or 3). When three or more sample replicates are used to derive the analytical result, the type A uncertainty is the standard deviation of the mean value (S/?n), where S is the standard deviation of the derived results. The type B uncertainties are all other random or non-random components that are not included in the standard deviation. The derivation of the general "Lawof Propagation of Errors" equations and specific example are available on TestAmerica rptGeneralInfo \'3.72 TestAmerica Laboratories, Inc. 4 o. Report No. : 53660 Client Id Batch Work Order Parameter 2283081 FFSR R1 Baghouse Filter(6038)/Bkr MWTWE1A U-234 U-235 U-238 R2 NYC Filters (6039;6040)/Bkr MWTWK1A U-234 U-235 U-238 2306033 FFSR R1 NYC Filters (6037) I Beaker MWTWJ3A U-234 U-235 U-238 No. of Results: 9 Sample Results Summary TestAmerica Ordered by Method, Batch No., Client Sample 10. Result +-Uncertainty ( 25) 1.53E-03 +-3.7E-04 9.04E-05 +-6.7E-05 1.42E-03 +-3.5E-04 2.81 E-02 +-7.2E-03 1.39E-03 +-4.4E-04 2.61 E-02 +-6.7E-03 3.55E-02 +-6.5E-03 1.00E-03 +-4.2E-04 3.35E-02 +-6.2E-03 Qual Units UCI/SA UCI/SA UCI/SA UCI/SA UCI/SA UCI/SA UCI/SA UCI/SA UCI/SA Date: 08-Nov-12 SOG No: 45792 Tracer Yield 99% 99% 99% 94% 94% 94% 108% 108% 108% MDL CRDL 4.20E-05 9.00E-15 5.27E-05 9.00E-15 5.27E-05 9.00E-15 5.33E-05 9.00E-15 4.49E-05 9.00E-15 4.49E-05 9.00E-15 1.35E-04 9.00E-15 1.35E-04 9.00E-15 3.34E-04 9.00E-'15 RER2 TestAmerica RER2 -Replicate Error Ratio = (S-D)/[sqrt(sq(TPlis)+sq(TPUd») as defined by ICPT BOA. rptSTLRchSaSum mary2 VS.2.22 A2002 TestAmerica Laboratories, Inc. 6 ) ·1 J QC Results Summary Date: 08-Nov-12 TestAmerica Ordered by Method, Batch No, QC Type,. Report No. : 53660 SDG No.: 45792 Batch Tracer LCS Work Order Parameter Result +-Uncertainty ( 2s) Qual Units Yield Recovery Bias MOL FFSR 2283081 BLANK QC, MWWAP1A U-234 1.28E-08 +-3.1 E-08 U UCI/SA 81% 6.99E-08 U-235 -1.23E-09 +-3.1 E-08 U UCIISA 81% 6.16E-08 U-238 -4.29E-09 +-3.1 E-08 U UCI/SA 81% 7.91 E-08 2283081 LCS, MWWAP2A U-234 2.15E-06 +-5.1 E-07 UCI/SA 87% 123% 0.2 8.42E-08 U-238 1.66E-06 +-4.2E-07 UCI/SA 87% 91% -0.1 6.13E-08 FFSR 2306033 BLANK QC, MW7AC1AA U-234 2.59E-08 +-3.7E-08 U UCI/SA 107% 4.72E-08 U-235 -1.56E-09 +-2.6E-08 U UCI/SA 107% 5.60E-08 U-238 -1.56E-09 +-2.6E-08 U UCI/SA 107% 5.60E-08 2306033 LCS, MW7AC1AC U-234 1.45E-06 +-3.7E-07 UCI/SA 104% 88% -0.1 4.71E-08 U-238 1.40E-06 +-3.6E-07 UCI/SA 104% 81% -0.2 4.71 E-08 No. of Results: 10 TestAmerica Bias -(Result/Expected)-l as defined by ANSI N13.30. rptSTLRchQcSum U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mal, Total Uncert, CRDL. RDL or mary VS.2.22 not identified by gamma scan software. A2002 TestAmerica Laboratories. Inc. 7 Lab Name: TestAmerica Lot-Sample No.: J2J040470-1 FORM I SAMPLE RESULTS Client Sample ID: R1 Baghouse Filter(6038)/Bkr Denison Mine 2012 3rd Quarter SDG: 45792 Report No. : 53660 COC No.: Parameter Batch: 2283081 U-234 U-235 U-238 No. of Results: 3 Result Count Qual Error ( 2 s) FFSR 1.53E-03 2.7E-04 9.04E-05 6.5E-05 1.42E-03 2.6E-04 Comments: Total MDL, Rpt Unit, Yield RstlMDL, Uncert( 2 s) Action Lev Lc CRDL(RL) RstlTotUcert Work Order: MWTWE1AA Report DB 10: 9MWTWE10 3.7E-04 4.20E-05 UCI/SA 99% (36.5) 5.37E-06 9.00E-15 (8.2) 6.7E-05 5.27E-05 UCI/SA 99% (1.7) 1.07E-05 9.00E-15 (2.7) 3.5E-04 5.27E-05 UCI/SA 99% (26.9) 1.07E-05 9.00E-15 (8.) U-2341238 = 1.1 Date: 08-Nov-12 Collection Date: 9/28/2012 11 :00:00 AM Received Date: 10/4/2012 10:00:00 AM Matrix: FILTER Ordered by Client Sample 10, Batch No. Analysis, Prep Date 10/26/12 05:56 p 10/26/1205:56 p 10/26/12 05:56 p Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.00107 Sample 0.00107 Sample 0.00107 Sample Primary Detector ALP10 ALP10 ALP10 TestAmerica MDClMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.2.22 A2002 TestAmerica l.aboratories, Inc. 8 Lab Name: TestAmerica Lot-Sample No.: J2J040470-2 FORM I SAMPLE RESULTS Client Sample 10: R1 NYC Filters (6037) / Beaker Denison Mine 2012 3rd Quarter SDG: 45792 Report No. : 53660 COC No.: Parameter Batch: 2306033 U-234 U-235 U-238 No. of Results: 3 Result Count Qual Error ( 2 s) FFSR 3.55E-02 2.3E-03 1.00E-03 3.8E-04 3.35E-02 2.2E-03 Comments: Total MOL, Rpt Unit, Yield RstlMDL, Uncert( 2 s) Action Lev Lc CRDL(RL) RstlTotUcert Work Order: MWTWJ3AA Report DB 10: 9MWTWJ30 6.5E-03 1.35E-04 UCI/SA 108% (263.2) 1.72E-05 9.00E-15 (10.9) 4.2E-04 1.35E-04 UCI/SA 108% (7.4) 1.72E-05 9.00E-15 (4.7) 6.2E-03 3.34E-04 UCI/SA 108% (100.5) 1.17E-04 9.00E-15 (10.9) Ratio U-2341238 = 1.1 Date: 08-Nov-12 Collection Date: 9/28/2012 11 :00:00 AM Received Date: 10/4/2012 10:00:00 AM Matrix: FILTER Ordered by Client Sample 10, Batch No. Analysis, Prep Date 11/6/1202:25 p 11/6/12 02:25 P 11/6/1202:25 p Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.00035 Sample 0.00035 Sample 0.00035 Sample Primary Detector ALP211 ALP211 ALP211 TestAmerica MDClMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. VS.2.22 A2002 TestAmerica Laboratories. Inc. 9 Lab Name: TestAmerica Lot-Sample No.: J2J040470-3 FORM I SAMPLE RESULTS SDG: 45792 Report No. : 53660 Client Sample 10: R2 NYC Filters (6039,6040)/Bkr Denison Mine 2012 3rd Quarter COC No.: Parameter Batch: 2283081 U-234 U-235 U-238 No. of Results: 3 Result FFSR 2.B1E-02 1.39E-03 2.61E-02 Comments: Count Qual Error ( 2 s) 1.2E-03 2.6E-04 1.1 E-03 Total MDL, Rpt Unit, Yield RstlMDL, Uncert( 2 s) Action Lev Lc CRDL(RL) RstiTotUcert Work Order: MWTWK1AA Report DB ID: 9MWTWK10 7.2E-03 5.33E-05 UCI/SA 94% (526.6) 9.95E-06 9.00E-15 (7.8) 4.4E-04 4.49E-05 UCI/SA 94% (31.) 5.75E-06 9.00E-15 (6.3) 6.7E-03 4.49E-05 UCIISA 94% (581.5) 5.75E-06 9.00E-15 (7.8) Ratio U·2341238 = 1.1 Date: 08-Nov-12 Collection Date: 9/28/2012 11 :00:00 AM Received Date: 10/4/2012 10:00:00 AM Matrix: FILTER Ordered by Client Sample 10, Batch No. Analysis, Prep Date 10/26/1205:57 p 10/26/1205:57 p 10/26/1205:57 p Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.00099 Sample 0.00099 Sample 0.00099 Sample Primary Detector ALP12 ALP12 ALP12 TestAmerica MDCIMDA,Lc • Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual· Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. VS.2.22 A2002 TestAmerica Laboratories. Inc. 10 FORM II Date: 08-Nov-12 BLANK RESULTS Lab Name: TestAmerica SDG: 45792 Matrix: FILTER Report No. : 53660 Count Total MDL, Rpt Unit, RstlMDL, Analysis, Total Sa Aliquot Primary Parameter Result Qual Error ( 2 s) Uncert( 2 s) Lc CRDL Yield RstlTotUcert Prep Date Size Size Detector Batch: 22B30B1 FFSR Work Order: MWWAP1AA Report DB 10: MWWAP1AB U-234 1.2BE-OB U 3.1 E-OB 3.1 E-OB 6.99E-OB UCI/SA B1% 0.1B 10/26/1205:56 p 1.0 1.0 ALP71 1.43E-OB 9.00E-15 0.B3 Sample Sample U-235 -1.23E-09 U 3.1 E-OB 3.1 E-OB 6.16E-OB UCI/SA B1% -0.02 10/26/12 05:56 p 1.0 1.0 ALP71 1.01 E-OB 9.00E-15 -O.OB Sample Sample U-238 -4.29E-09 U 3.1 E-OB 3.1 E-OB 7.91 E-OB UCI/SA B1% -0.05 10/26/12 05:56 p 1.0 1.0 ALP71 1.B9E-OB 9.00E-15 -0.2B Sample Sample Ratio U-2341238 = -3.0 -------------.. -----------.-----.. -.--.----------------- Batch: 2306033 FFSR Work Order: MW7AC1AA Report DB ID: MW7AC1AB U-234 2.59E-OB U 3.7E-08 3.7E-08 4.72E-08 UCI/SA 107% 0.55 11/6/1202:25 p 1.0 1.02 ALP212 6.03E-09 9.00E-15 (1.4) Sample Sample U-235 -1.56E-09 U 2.6E-08 2.6E-08 5.60E-08 UCI/SA 107% -0.03 11/6/1202:25 p 1.0 1.02 ALP212 1.04E-08 9.00E-15 -0.12 Sample Sample U-238 -1.56E-09 U 2.6E-OB 2.6E-OB 5.60E-08 UCI/SA 107% -0.03 11/6/1202:25 p 1.0 1.02 ALP212 1.04E-08 9.00E-15 -0.12 Sample Sample Ratio U-2341238 = -16.7 ------------.. ---~.----.---------------- No. of Results: 6 Comments: TestAmerica MDCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchBlank lJ Qual -Amtlyzed for but not detected above limiting criteria. Limit criteria is less than the I\1dc/lVlda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.2.22 A2002 TestAmerica Laboratories. Inc. J I Lab Name: TestAmerica Matrix: FILTER Parameter Result Qual Batch: 2283081 FFSR U-234 2.15E-06 U-238 1.66E-06 Batch: 2306033 FFSR U-234 1.45E-06 U-238 1.40E-06 -- No. of Results: 4 Comments: Count Error ( 2 s) 3.5E-07 3.1 E-07 2.7E-07 2.7E-07 Total Uncert( 2 s) MOL FORM II Les RESULTS Report Unit Yield Expcctcd Expected lJncert Work Order: MWWAP2AC Report DB ID: MWWAP2CS 5.1 E-07 8.42E-08 UCI/SA 87% 1.75E-06 9.57E-09 Ree Limits: 75 125 4.2E-07 6.13E-08 UCI/SA 87% 1.83E-06 1.00E-08 Ree Limits: 75 125 --_. __ ._---------------_. __ .. __ ._------ Work Order: MW7AC1AC Report DB ID: MW7 AC1 CS 3.7E-07 4.71E-08 UCI/SA 104% 1.65E-06 9.06E-09 Ree Limits: 75 125 3.6E-07 4.71 E-08 UCI/SA 104% 1.73E-06 9.49E-09 Ree Limits: 75 125 -----_.---_._---------------------_.- TestAmerica rptSTLRchLcs VS.2.22 A2002 Bias -(RcsuJt/Expected)-1 as defined by ANSI NI3.30. Testl\merica Laboratories. Inc. 12 Date: 08-Nov-12 SDG: 45792 Report No. : 53660 Rccovcry, Analysis, Aliquot Primary Bias Prep Date Size Detector 123% 10/29/12 12:21 p 1.0 ALP4 0.2 Sample 91% 10/29/1212:21 p 1.0 ALP4 -0.1 Sample -----. __ .. "---_._-_ .. 88% 11/6/12 02:26 p 1.04 ALP213 -0.1 Sample 81% 11/6/12 02:26 p 1.04 ALP213 -0.2 Sample -----------------------.-. --i (1) (fJ ;; 3 (1) :1. n s::.:> r ~ o! ~ ~. ;n 5" fl vol ~:.~ .: . .-:'. {~) ,~ .. :~ ~I.~' I';~f~~'~:.~'~;' · .. t:;':;;~i~::.:.~l:}/I~:.::::!.~~:;'~ Chain of Custody Record TAl..-4l24 (lOO7) Client Temperature on Rec(;!ipt __ _ TestAmerica Drinking Water? Yes 0 No 0 THE LEADER IN ENVIRONMENfAL TESTING Pro/eet Mans.oar Date Tetco Dean Kitchen i 10/01/2012 I I,CI78.il1..oICu.s£odtt Number. Address; .. -.. -.... -... -... -.. --.. -. -. -',.:-.-,--'..,..".,-,.--. -.-. -.. ---.,-... -.. -.. -.... -:-:: ... : .. 18Jephone NUmbGr {Area. Code)IFax Number Lab Number " i 391 East 620 South . : 801:A92~9106. Page__ 1 of / City ... ..... • ..... ... ... .4JP .COQI! ... -.-siie C~~cr . . .. . Lab Contacc Anafysis (Attach list if American Fork ... 84003.. Scott Christensen, Garren Palmer more space [$ needod) Profcr;f N~me and Location {State) Denison Mine 20111st Quarter Conuact/PUrc!Ia9& Order(Quoto No. CfmieoWaybm Number Matrix Containers & Preservatives Sampfe I.D. No. and Description ! Date Time ~ rl _ leg (3 _ es ~~ 0 °1 ~I ~ <fl. N. '. rol N N -0. ~i :6; rU m :::>' f-" cc ...J. Special lnstructions/ Conditions of Rece;pt (Containers tor each "amp'e may M combfned on on9line) I ~ ~ :~ ~ i ~ ~ ~ ~ ~ ~~ r-'" ........ -._-----.1"':::++--1--'-+-++--1-+-+-+-+. -f-+-+-+---------- 'R1 Baghouse filter (6038) and beaker ., 10/28/12. [11:00 X 1. X.! . ____ ! Y'<1~w-E: .... : R1 NYC filters (6037) and beaker J .10./28/12 ..IlB:OO . Xi X i I \IV\. u..)\ 0"5 : R2 NYC filters (6039,6040) and beaker 10/29/12 8:00 X X .. I VV\~\\..0\( l I I ~~ .. D~s:?:i':"\ D . .. . ~\~~'-\~~(~ra . .... ....... .... I 'l:)~>(.." . \\-:-:-\ \d-... . -l~--I-l-' I I I 1111111111111111111111111111111 J2J040470 ! i ! i I I ~~~~ __ ~~~~~ __________________ ~ __________ -L ______ ~-r,~=7.~~~~~~ __ ~~ __ .L-~ __ ~~~~ __ L~-~~- Possible Hazard Identification Sample Disposal. '. (A fee may te BS$$$3ed if semp(es ere retained o Non·Hazard 0 FJammabre 0 Skin /rril8r1t 0 Poison!3 . 0 Unknown 0 Rft/am To Client ~ Dlsposa( By Lab 0 Archive For ___ Months longer tha.n 1 month) Tum Around Ttme Required I ac: Requirements (Specify) o 24 Hour~.,,"\ 0 48 Hours 0 7 Days 0 14 Days 0 21 Days 0 other as oermethod ..... 1. Rsce/V9d By -:-:::--""~--":'~ ~\'L ~ 2. Rece{ved By '<3L~ Time -- 1. Rerlflql~~!Jed J: 7 ( l,-~ .. l~t~ I J)! ! 1Tmq 2. Relinqu[;;}j;;, J -----.-...• , oaie--~·-:-fL~ Time 2. Relinquished By Comments When Complete Email to:DeanorPaultetco@tetco-ut.com D1STRIBUWN; WHii'E; -Re!Umeri to Cliellt with Report; CANARY-Stays with the Sample; PINK -Fl<Jld Copy TestAmerica L THE .. fiADEn IN C:NVlrWNMENTAL TESTING Date/Time Received: \p .... \.\-\1,... \ l60V \ Sample Check-in List Container GM Screen Result: (Airlock) to ¥ Samplc GM Screen Result (Sample Receiving) 1#' Llt) Client: c'06o SDG #:3S_~~_~ ____ NA [] SAF #: Initial~ ] _Initials~ ] ____ N~ Lot Number: ~d~O~OWV\O Chain of Custody it -------.------.... -----------------------~------ Shipping ContainerID: N~ Air Bill Number: NA~ Samples received inside shipping container/cooler/box Yes~ ] Continue with I through 4. Initial appropriate response. No [ ] Go to 5, add comment to #16. l. Custody Seals on shipping container intact? Yes [ No [ No Custody Seal ~ ] 2. Custody Seals dated and signed? Yes [ No [ No Custody Seal ~ 3. Cooler temperature: ___ oC NA (l~ ] 4. Vermiculite/packing materials is NA[ Wet[ 1 D~ Item 5 through 16 for samples. Initial appropriate response. 5. Chain of Custody record present? Yes'~ ] No [ 6. Number of samples received (Each sample may contain multiple bottles):_-_') ______________ _ 7. Containers received: /")'l .~~i \\04..-', ~ i bQA ~ 8. 9. 10. 11. Sample holding times exceeded? Samples have: __ tape __ custody seals Matrix: ~A (FLT, Wipe, Solid, Soil) __ oS (Air, Niosh 7400) Samples: C\~ A are in good condition I'--are broken NA[ Yes [ hazard labels 3f=appropriate sample labels __ T (Water) __ T (Biological, Ni-63) __ are leaking NO~ ] ___ have air bubbles (Only for samples requiring no head space) Ofuer ______________________________________ _ 12. Sample pH appropriate for analysis requested Yes [ ] No [ ] NA (jl ] (If acidification is necessary, then document sample ID, initial pH, amount of HN03added Ynd pH after addition on table overleaf) RPL ill # of preservative used : _______________________________ _ 13. Were any anomalies identified in sample receipt? Yes [ ] No ~ ] lA. Description of anomalies (include sample numbers): NA \bl---------------------- LS-023,Re~ 15,07/11 See over for additional information. TestAmerica Laboratories, Inc. 14 J TestAmerica THE l.EAI)(;Ft IN ~NVlrWNM(;NTAL TESTINO 15. Sfimple Locatiori,. \,s~aH1ple Collector Listed on COC? * *For documentation only. No COITective action needed. Yes~ ] No [ 16. Additional InfOrl11atiOn:_ .. ~~, 10 ~.<:.~~J.,......!...:.. _____ . [ ] Client/Courier denied temperature check. ] Client/Courier unpack cooler. Sample Custodian: t -: ~ Client Informed on S ... ---' '2--by c!>4MM 1 Date: \ (') .,':-\-\~ Person contacted '~ i~'~o action necesser' proces: as is Project Manager GLl J. 1.<>.< ~ Date 'J o--s--r~ SAMPLEID Initial pH Acid Amt Final pH ~AMPLEID Initial pH Acid Amt \ \ '\ '\ \ '\ \ \ \ \ \ \ \ \ \ \ 1\ \ VI \ .. _7) ~ c~ V \( ~ , \ ~> \7 r) K\. \~ \~ \(j \ \ \ \ \ \ \ \i \ \- \ \ Final pH I \ \ \ \ \ LS-023, Rev. 15,07/11 See over for additional information. TestAmerica Laboratories, Inc. 15 APPENDIXD North Yellow Cake Scrubber Figure 1. Facility Schematic Representation Yellow Cake Dryer Baghouse Figure 2. Facility Schematic Representation Process Data (Retained by Energy Fuels Resources) D ~. .. Facility: eniSOn MIneS t a ! y Stack Identification: ·NorthYellow Cak.e Scrubber 1~0~1 ~ a: Distance upstream from next disturbance, feet ~: Distance downstream from last disturbance, feet y: Distance of Sample Level to Ground, feet 0: Stack Inside Diameter, inches Estimated Moisture, percent Estimated Temperature, OF Estimated Velocity, fpm Control Unit Type: Scrtlbber Number of Ports ~ 9.5' ------------------- 9.5' 65' ------------------ 18" ------------------ 8-15%) 100-120 ------------------ 1.100 ------~---------- 'I 4- Figure 1. Facility Schematic Representation Process Type: Yellc)\v Cake Processing Facility: Denison JV11neS t a ! y Stack Identification: Yell()w Cal<eDryerBa,gho'use 1~0~1 , a p a: Distance upstream from next disturbance, inches p: Distance downstream from last disturbance, inches y: Distance of Sample Level to Ground, feet 0: Stack Inside Diameter, inches Estimated Moisture, percent Estimated Temperature, of Estimated Velocity, fpm Control Unit Type: Baghouse Number of Ports ~ 57" -------------------- 45411 65' ------------------ 16" ------------------- 0-2% 125 ------------------- 1.400 --------~-------- 2 Figure 2. Facility Schematic Representation Process Type: Yellow Cake Processing Energy Fuels Resources, Blanding, UT Process Data Source: North Yellow Cake Date: Time l S - /IJ I. I \ ( c;- \. .7 Ie; I~( l ! r I \.( i~ 'J -'J Scrubber Flow GPM #1 #2 L. &. J \ ! Z· /.J I( " 7 I \ \ I...-. • Ie {./ S G I z· (J i1P /./ f [' ,I o '--I i L(.O c( (J L(, / l(, / y.' / J Energy Fuels Resources, Blanding, UT Process Data Source: North Yellow Cake Date: c;,'7/' 17 ,I 'L.-'1 ; C Scrubber Flow GPM Time #1 '1 S' ....--: --r-' 0 .-""~ v- I ,-"'I I :s c---; ---u -I ~/-(~ c) ,,;-----'j :::> ~~ > u s- c 1 (j 0 C;, --1 1'- /"' ?(») s-> '---1 (~ C) t;;; ~ \ 0 { 0 ')0 C,-Cl J /\ C:' ~" l- l ( \J 0 J 1 I '7 s-(1 '/ () ~ VI ! 7 <-/ ,~) "-,~ '-_ ..... \. ( L .5 , ~ S \ c-S I 7 C' (~ ( I / -../ U ,Y ! -; S-' c--) j L-" 1 J " 1 c: L /- ~ ! \ \.,1 -; [' c;-c:::, \ 5 1 s: (/ -- --- S' --:/ ('/-( ) L> \. ; J >' #2 2_ I ( I Z \ ( i I!l. Z (J 1 ! c-r I I, L, l ~ -; (.-I / I 7 c;;--L I Z L, 1 C ; l· ) /7 7 t L.. '-I 7 /1 v !,../ , ) ? ~ ( ./ I--z, Z j ~, , 7 c. 7 L , " I I c> i .--; ( I ; ~P I I L--! . 4.i I I I ---j. U L(. (J L/'6 , (~ u, ' , u l/, APPENDIXE Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature sensors were carried out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 3 Schematic of Method 51114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-test Dry Gas Meter Calibration Data Forms Type S Pitot Tube Inspection Data Sample Box Temperature Sensor Calibration E Temperature Sensor t ~prObe Type S Pilot Tube Temperature Nozzle tb:i:T!'a:;OO sensor~ Gooseneck ! ~ (3a;s.lirai / Pn:be -~ / Type S Pitot Tube ~ Temperature Sensor Glass FiJter Holder Heated Area Impinger Train Optional. May Be Replaced B)' An Equivalent Condenser I Temperature Sensor ,-- --.-- -------- Impingers Stack Wall Manometer Temperature Sensors .. Air-Tight Pump Figure 3 Schematic of Method 5/114 Satnpling Train METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES ~ .f~ 9 _MIU __ !!I1iI'1ii!j1 Ii-=iI 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report). for a period of time necessary to achieve a minimum total volume of 5 cubic feel. 4) Record data and information in the cells. YELLOW cells are calculated. METER SERIAL #:If-"':'::':==-=-- CRITICAL ORIFICE SET SERIAL #: .1...-.., ___ -' EQUIPMENT JD #: G G G K' TESTED FACTOR I VACUUM RUN # , (AVG) (in Hg) 0.8137 13 0.8137 13 0.8137 13 0.5317 13 0.5317 13 0.5317 13 0.3307 13 0.3307 13 0.3307 13 548.140 553.420 558.698 564.820 570.025 575.265 581.802 587.303 592.812 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 553.420 5.280 75 73 558.698 5.278 75 73 564.244 5.546 75 75 570.025 5.205 75 76 575.265 5.240 75 80 580.513 5.248 75 81 587.303 5.501 75 84 592.812 5.509 75 86 598.325 5.513 75 87 73 73 75 76 76 80 80 82 81 84 83 85 86 88 87 86 89 87 76 80 83 84 85 87 86 87 89 ENVIRONMENTAL SUPPLY COMPANY Facility New Calibration 2012 INITIAL FINAL AVG(Pbar) 25.30 25.3 IF YVARIATION EXCEEDS 2.00%. ORIFICE SHOULD BE RECAll BRA TED ELAPSED 1 ::l TIME (MIN) AVG e 73.75 4.4546 4.4515 0.999 76 ~ 4.4515 1.004 78.50 ~ 4.6740 1.008 AVG= 1.004 .0.22 80.50 7.50 1.20 4.3152 4.3631 1.011 82.50 7.50 UO llill lllli 1.:QQ! 84.00 7.50 1.20 4.3229 4.3631 1.009 AVG= 1.009 Qd2 86.00 § ~ ~ 1.004 86.50 0.44 4.5072 4.5229 1.003 88.00 0.44 4.4981 4.5229 1.006 AVG= 1.004 .0.15 The following equations are used to calculate the standard volumes of air passed through the DGM. V m (std). and the critical orifice. V CI (std). and the DGM calibration factor. Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR. Y = I 1.006 (1) (2) (3) VtII,.",/) '= K, * VII1 * ['hal" + (L\H / 13.6) Tm l'ha,. * e J ·c,.(",,,) ~c K'* JT£lmh = Net volume of gas sample passed through DGM. corrected to standard conditions Kl = 17.64 OR/in. Hg (English). 0.3858 °Klmm Hg (MetriC) T m = Absolute DGM avg. temperature (OR -English. OK -Metric) = Volume of gas sample passed through the critical orifice. corrected to standard conditions Tamb = Absolute ambient temperature (R -English. OK -Metric) K' = Average K' factor from Critical Orifice Calibration VCI;."dJ "'111,,,,,) = DGM calibration factor Pre Calibration 2008 AVERAGE ~H@ =1 1.641 2 ~H@ = ( 0.75 e) ~H (Vm(std)\ Vcr(std) Vm J Temperature Sensors Reference In Out OF OF OF 34 67 202 35 68 203 35 68 203 1.736 1.729 1.721 ~ lSI .l,ffi 1.548 1.547 1.542 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES r-~ UiH1WWMPifa'&@rtiWw; .-,..--9 """"" ;;;;!i'.":,~ 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the cells, YELLOW cells are calculated. METER SERIAL #:1-1 ___ ~ CRITICAL ORIFICE SET SERIAL #: .... ' ___ ...... EQUIPMENT 10 #: K' TESTED r--------r----~I FACTOR I VACUUM o G G RUN # I (AVG) 0.8137 0.8137 0.8137 0.5317 0.5317 0.5317 0.3307 0.3307 0.3307 (inHg) 12 12 12 12 12 12 12 12 12 329.8090 337.470 345.174 295.10 300.815 306.502 312.5510 317.867 323.241 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 337.470 345.174 352.898 300.815 306.502 312.205 317.867 323.241 328.625 7.661 7.704 7.724 5.715 5.687 5.703 5.316 5.374 5.384 68 92 68 93 68 94 70 80 70 81 70 82 70 82 70 85 70 88 93 89 94 96 95 98 82 85 82 86 86 88 -- 83 85 87 86 89 86 91 97 100 86 88 89 86 87 91 INITIAL FINAL 25.55 ELAPSED TtME(MIN) e r--- 91.25 7.00 95 7.00 96.75 7.00 83.25 8.00 84.25 8.00 86.25 8.00 L..---- 84.00 12.00 86.25 12.00 88.50 12.00 t:1'iVI~UI'iIVIt:I'i I.f\L ~Ut"t"L T \"UIVIt"AI'i T AVG (Pba,) 25.55 3.10 3.10 3.10 B: 1.25 0.47 0.47 0.47 2012 Pre-Calibration Console 7 2dill §d1fi 6.3121 4.7612 Qill ~ 4.4128 4.4425 4.4325 IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED ! 6.3353 ~ ~ '1.003 6.3353 1.004 AVG= 1.003 0.49 4.7221 0.992 4.7221 !ill! 4.7221 0.999 AVG= Q.&ll ::ll.:.ll 4.4055 0.998 4.4055 0.992 4.4055 0.994 AVG= 0.995 -0.34 :L.ill. 1.745 1.740 1.681 1.678 !:§ll 1.628 !:.ill 1.615 The following equations are used to calculate the standard volumes of air passed through the DGM, V m (std), and the critical orifice, Vcr (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 0.998 (1 ) (2) (3) VII1I.",/) = K,* Vm '" Pbar+ (M! 113.6) [,har * 0 Vcr(.w/) = K'* .JTamh = Net volume of gas sample passed through DGM, corrected to standard conditions Kl = 17.64 aRlin. Hg (English), 0.3858 °Klmm Hg (Metric) T m = Absolute DGM avg. temperalure (OR· English, OK -Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions Tamb = Absolute ambient temperature (OR -English, OK -Metric) K' = Average K' factor from Critical Orifice Calibration J'CI;.;,d) r--= DGM calibration factor -r'/11I.:''/) AVERAGE ~H@ =1 f.682 L'lH@= (0.750)2 ~H (Vm(std)) Vcr(std) Vm Temperature Sensors Reference In Out OF 32 72 201 OF 33 73 202 OF 33 73 203 7 console Pre 2012 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES lie: inmUMi§4§i§Gid@.t/""1iji' --<i~~~ t.r ' ,," 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. ENVIRONMENTAL SUPPLY COMPANY 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated. METER SERIAL #: CRITICAL ORIFICE SET SERIAL #:1-1-1-4-53-S--; EQUIPMENT ID #: K' TESTED RUN# I FACTOR I VACUUM (AVG) (in Hg) O:EEd ~ .0 I I ] II] .0 .0 0: 0.6808 13 0.6808 13 0.6808 13 830.903 836.165 836.165 841.465 841.465 847.20 5.262 70 74 75 78 80 70 75 77 80 82 70 77 78 82 82 5.30 5.735 O:EEd ~ .0 I I III I .0 .0 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: DGM AVG o o 0.00 76.75 78.50 79.75 0.00 0.00 0.00 Facility FINAL AVG (Pb.,) 25.60 ELAPSED TIME (MIN) e 25.60 §§ 6.00 2.00 6.00 2.00 6.50 2.00 §§ Energy Fuels 4.4551 4.4727 4.8285 IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 1 AVG= 4.5436 1.020 4.5436 1.016 4.9222 1.019 AVG= 1.018 0.00 AVG= The following equations are used to calculate the standard volumes of air passed through the DGM, Vm (std), and the critical orifice, V CT (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 1.018 (1) (2) (3) Vm(std) = K j *Vm* Pbar+(f..H /13.6) Tm Pbar '" 0 K'* --.-=-~ Veres/d) = ~mh = Net volume of gas sample passed through DGM, corrected to standard conditions Kl = 17.64 OR/in. Hg (English). 0.3858 °Klmm Hg (Metric) T m = Absolute DGM avg. temperature (OR -English. OK -Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T.mb = Absolute ambient temperature (OR -English, OK -Metric) K' = Average K' factor from Critical Orifice Calibration Vcr(sld) y = ---= DGM calibration factor Vm(sld) Pre Calibration 2008 AVERAGE AH@=C 1.656 2 AH@ = (0.75 e) AH (Vm{std)) Vc,{std) Vm Temperature Sensors Reference In Out OF 34 67 202 OF 35 68 203 OF 35 68 203 1.661 1.656 1.652 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES ~ ummwi§4§iiW@ldtnm,-r---~'~i -~'~.;' -~-::" -.... iOO * -;!;~~;,c-Af' 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated. METER SERIAL #: CRITICAL ORIFICE SET SERIAL #: 1-1-1-4-53-S-" K' I TESTED ,-----.,----11 FACTOR I VACUUM RUN # I (AVG) (in Hg) .0 D:rn~ .0 .0 EJ: 0.5317 12 0.5317 12 0.5317 12 786.10 791.746 ,!97.416 791.746 797.416 803.070 5.646 5.670 5.654 EQUIPMENT ID #: 1-TI 70 78 70 78 70 80 INITIAL Console #7 ::l AVG r-ll 0 0 0 78 81 83 80.00 80 83 87 82.00 82 87 90 84.75 :II r::.l"VI~UI"IVlr::.l" IRL \:)UrrL T \"UIVlrRI" T Energy Fuels Resources FINAL AVG (Pbar) 25.45 25.45 IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED ELAPSED I 1 I TIME ~MIN) I r=:l § § AVG= 8.00 1.25 4.7136 4.7036 0.998 8.00 1.25 4.7161 4.7036 0.997 8.00 1.25 4.6791 4.7036 1.005 AVG= 1.000 0.00 D:rn~ §§ .0 II I I I I 0.00 0.00 .0 0.00 .0 AVG= USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: The following equations are used to calculate the standard volumes of air passed through the DGM, Vm (std), and the critical orifice, Vcr (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 1.000 (1) (2) (3) Vm(std) =K\ *Vm*Pbar+(M-{/13.6) Tm l'har * e -K'*---~=-Vcr(Sf") -..J1'amh = Net volume of gas sample passed through DGM, corrected to standard conditions Kl = 17_64°R/in_ Hg (English), 0_3858 °Klmm Hg (Metric) T m = Absolute OGM avg_ temperature (OR -English, oK -Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions Tamb = Absolute ambient temperature (OR -English, OK -Metric) K' = Average K' factor from Critical Orifice Calibration VC1(~/d) Y = ---= DGM calibration factor Vm(sld) AVERAGE AH@=(--1.691 2 AH@ = (0.75 e) AH (Vm(std)) Vc,(std) Vm Temperature Sensors Reference In Out OF 32 72 201 OF 33 73 202 OF 33 73 203 1.698 1.692 1.683 7 console Post 2012 APPENDIXF The testing followed the same procedures as outlined in previous protocols and tests at this facility. Type S Pitot Tube Inspection Data (l., -YL-1 \ Date. Pitot Tube Identification: __ ~--,-_ .. _'---"Js:"'--_____ _ at Technician: __ K~,-,-. ..&.'-1'I-\J\:::..;...~k~tJ...:..:....t-..."":::"-lML=-.~(t..!A.~\.!..-.:<A-=-=:.....-___ _ ~ ~ .. PA A 1 , a • f'B I ., I Dr-• .:s I. ( in. p ... == • 4 ~b in. ~---~~------- PB'"" • l{ (0 in. ~--~-~~--- 01 == ___ v~=---__ 02 < 5° 02 == ___ '---__ z ~ 0.125 in. Z= .OOt in. W::; 0.03125 in. W= 00 ~l in W > 3 inches W= (ok in Z> 3/4 inch Z= lh: 11 in. y ~ 3 mches The Pltot tube meets the specificatIOns for a caltbration factor oro 84<) '1.e~ Temperature Sensor Calibration Rcfercnct? Temperature Temperature I T em perature Source Reference Sensor Dlff~rence (\-1cdlUm) rF) ("F) ('F) AIR (pC ~t1 I Probe Contmulty -, y.e,..!> He3t Che-=k ~~8 i-/ \t<...j 1.'60 AIR ~~ cpt.( , i ICE WATER I '"$."1-31 -t StacK BOIL W:HER ,.,0,.., ~o t \ SILICONE OIL Type S Pitot TlIb~ InspcLtion Dat:l Dt= .'3] S In. G....l-~ -------- r -p --P ') ".J (I .~ .-\ -B -4=<:"'::::' p,,'-' • y t1 :> in. 15 1. 05 • D, ~ D, ::::; 1.50· Dc ? -'{4.-:<:--="~:1!>----- /01 " , --<~ ._--- L. ____ .. ~ ." " B \ -""""'-Z 62 ~-~'W -.··:....··_ .. -<.,,-.. 3 .. ·_··_ .. _ .. -· I J ~ '-::.-... '.1----""-,::,:={ :=:::::===.==-=:;::::-==='~~ C I: .. ,.., .. """. Q) i p~ == Ll L( :s in (L, < It)" ell == __ --->-__ _ (:.1 < 10° U: '" __ --"'0"'--__ 131= ___ L __ _ L ~ 0125 in W::;OO3125irJ. \v = 00 9 in W> -' inch.:s 1,\' ;: .:1 In Z > 3/4 inch l-= \ in ~ -S/ y '" ____ 'i.+-_I:1 ________ --.:...Tc:::.ri:2'fcfJ:ur;: Sensor C'alibr,ltJon R~tcrcn-:;:: . .---------- TETCO Sample Box Temperature Sensor Calibration Date: 12/29111 Calibrator: Kawai McNamara Unit ID A B c D E F ------------------------------~--- Thermocouple Location Oven Probe Out Impinger Out Oven Probe Out Impinger Out Oven Probe Out Impinger Out Oven Probe Out Impinger Out Oven Probe Out Impinger Out Oven Probe Out Impinger Out Impinger Out G Impinger Out H Impinger Out I Impinger Out J Impinger Out K Temperature Source Reference: Omega CL3512A Temp. Diff. or Result Prepared for: Energy Fuels Resources 6425 S H,vy 91 Blanding, Utah 84511 Date of Report: January 8, 2012 FOURTH QUARTER RADIONUCLIDE EMISSIONS TEST CONDUCTED AT ENERGY FUELS RESOURCES NORTH YELLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE GRIZZL Y BAGHOUSE BLANDING, UTAH November 26-28, 2012 by: TETCO 391 East 620 South American Fork, UT 84003 Phone (801) 492-9106 Fax (801) 492-9107 fax CERTIFICATION OF REPORT INTEGRITY Technical En1issions Testing Company (TETCO) certifies that this report represents the truth as well as can be derived by the methods en1ployed. Every effort was made to obtain accurate and representative data and to con1ply with procedures set forth in the Federal Register. Dean Kitchen ///J~,.J_ ~/~ Reviewer: ~~ /' tv" --------------~~~--~--.~------ Date: ________ .:..-I_--fJ-p'----....:...,/~)-- Mike McNamara ~/ t" I Revie\ver: I'.'}) 'f' 't--"··",,·· .. - ----~----~---------------------- ... Date: tJ . ~~ '-'I -\ .:; ------------------------------------- ji TABLE OF CONTENTS PAGE Introduction Test Purpose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Test Location and Type of Process .......................................... 1 Test Dates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Pollutants Tested and Methods Applied ...................................... 1 T P .. ? est artlclpants ......................................................... _ Deviations Fronl EPA Methods ............................................. 2 Quality Assurance ....................................................... 2 Sunllnary of Results Enlission Results ........................................................ 3 Process Data ............................................................ 3 Description of Collected Samples ........................................... 3 Discussion of Errors or Irregularities ......................................... 4 Percent Isokinetics ....................................................... 4 Source Operation Process Control Devices Operation .......................................... 5 Process Representativeness ................................................ 5 Sanlpling and Analysis Procedures Sampling Port Location ................................. ~ ................. 6 Sampling Point Location .................................................. 6 Sanlpling Train Description ................................................ 7 Sampling and Analytical Procedures ......................................... 7 Quality Assurance ....................................................... 7 Appendices A: COlnplete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence iii Table I II III IV V VI Figure LIST OF TABLES PAGE Measured Radionuc1ide En1issions .......................................... 3 Percent Isokinetics ....................................................... 4 Sampling Point Location .................................................. 6 Con1plete Results, South Yellow Cake Scrubber ...................... Appendix A Con1plete Results, Yello\v Cake Dryer Baghouse ...................... Appendix A Complete Results, Grizzly Baghouse ................................ Appendix A LIST OF FIGURES 1 Facility Schen1atic Representation South Yellow Cake Scrubber .......... Appendix D 2 Facility Schematic Representation Yellow Cake Dryer Baghouse ......... Appendix D 3 Facility Schematic Representation Grizzly Baghouse ................... Appendix D 4 Schematic of Method 51114 Sampling Train . . . . . . . . . . . . . . . . . . . . . . . . . . Appendix E iv INTRODUCTION Test Purpose This test project \vas conducted to determine the total radionuclide emissions from the South Yellow Cake Scrubber, Yellow Cake Dryer Baghouse, and Grizzly Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dscf). These tests were for U-Nat and Th-230 on the Grizzly Baghouse and U-Nat, Th-230, Ra-226, and Pb-210 on the South Yello\v Cake Scrubber and Yello\v Cake Dryer Baghouse. Test Location and Type of Process Energy Fuels Resources is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are t\VO yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Dryer Baghouse. The Packaging enclosure also discharges into the Dryer Baghouse. The South Yellow Cake (NYC) dryer was the only operating dryer at the time of the test. The North Yellow Cake Dryer w"as not operating at the tin1e of the test. The Grizzly Baghouse serve as the main dust control device for the raw ore unloading and conveying to the processing building. Stack schematics are shown as Figures 1 though 3 in Appendix D. Test Dates The first test run on the SYC Scrubber was split over three separate days, November 26-28. 2012. The reason for the split was production problems with the Dryer. The seco"nd test run \vas completed November 28,2012. One test run was completed on the Yellow Cake Dryer Baghouse November 28, 2012. One run w"as completed on the Grizzly Baghouse November 27,2012. Pollutants Tested and Methods Applied The tests w'ere a determination of radionuclide emissions in accordance \vith EPA Method 5/114. Test run filters and front wash residues were sent to Test America located in Richland. \Vashington for radionuc1ide analysis. Test Participants Test Facility State Agency TETCO Garren Palmer None Dean Kitchen Mike McNatnara Deviations From EPA Methods None Qualitv Assurance Doug Olsen Jeff Graton Testing procedures and san1ple recovery techniques were according to those outlined in the Federal Register and the Quality Assurance Handbookfor Air Pollution Measurement Systems. 2 SUMMARY OF RESULTS Emission Results Table I presents the findings of the test in Curies per dry standard cubic foot. Tables IV-VII in Appendix A have more detailed inforn1ation. Grizzly Baghouse 2 17.8 AVE 27.0 Process Data The process \vas operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flo\v, pressure drop readings (Llp) were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (Llp) were recorded and are found on the test run sheets. Production data is retrained bEnergy Fuels Resources. Description of Collected Samples The test filters for the South Yellow Cake Scrubber were heavily covered with an off-white colored particulate. The front washes \vere clear in appearance. The test filters for the Yellow Cake Dryer Baghouse were lightly colored with a tan colored particulate. The front wash was clear in appearance. The test filters for the Grizzly Baghouse \vere had no visible particulate. The front wash was clear in appearance. 3 Discussion of Errors or Irregularities None Percent Isokinetic Sampling Each of the tests \vere isokinetic within the ± 10% of 100% criterion specified in the Federal Register. They also meet the Utah State Department of Environmental Quality, Division of Air Quality specification of isokinetic san1pling point by point. Isokinetic values for each test run are presented in Table II. Table II. Percent Isokinetic Sam lina Run # 2 South Yellow Yellow Cake Cake Scrubber Dryer Baghouse 99 98 4 99 Grizzly Baghouse 99 SOURCE OPERATION Process Control Devices Operation All process control devices were operated normally. Recorded scrubber water flow, pressure and baghouse ilp readings were recorded and are found on the test run sheets or in Appendix D. Process Representativeness The facility was operated normally. Production data was retained by Energy Fuels Resources. 5 SAMPLING AND ANALYSIS PROCEDURES Sampling Port Location The inside diameter of the South Yellow Cake Scrubber stack is 12.75 inches. The t'NO~ four-inch dianleter sanlple port are located 28.24 diameters (30 feet) downstreanl from the last disturbance and 6.59 dianleters (7 feet) upstream fr01n the next disturbance. Figure 1 in Appendix D is a schenlatic of the stack. The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The tyVO~ four-inch dianleter sample ports are located 28.38 diameters (454 inches) downstream fr01n the last disturbance and 3.56 diameters (57 inches) upstream from the next disturbance. The sanlple port locations are depicted in Figure 2 in Appendix D. The inside dimneter of the Grizzly Baghouse stack is 18.75 inches. There are two, three-inch dianleter smnple ports located 2.56 dianleters (48 inches) downstream from the last disturbance and 1.31 dianleters (24.5 inches) upstreanl fr0111 the next disturbance. The sample port locations are depicted in Figure 3 in Appendix D. Sampling Point Location Table III shows the distance of each sampling point from the inside wall according to EPA Method 1. Each point is nlarked and identified with a wrapping of glass tape and numbered. These points are deternlined by nleasuring the distance fronl the inside "vall. Sample Point 2 3 5 6 7 8 9 10 11 12 Distance (inches) from Inside Wall NYC Scrubber 0 ouse Gri 0.85 3.19 9.56 11.90 6 0.70 2.34 4.74 11.26 ollse 0.50 1.26 2.21 3.32 4.69 6.68 12.08 14.06 15.43 16.54 17.48 18.25 Sampling Train Description To detennine the actual emission rates for this stack, 40 CFR 60, Appendix A, Methods 1-51114 were follo\ved. All saInpling trains were made of inert nlaterials, (Teflon, stainless steel and glass) to prevent interference of the sampled gas and particulate. The stack analyzers used to conduct Methods 1-51114 are constructed to lneet the specifications outlined in the CFR. The telnperature sensors are K-type thennocouples. Heater, vacuun1 and pitot line connections have been designed to be interchangeable with all units used by the tester. A 316 stainless steel probe liner was used for the tests. Figure 4 in Appendix E is a sketch of the Methods 51114 sampling train. Sample boxes \vere prepared for testing by following the prescribed procedures outlined in Methods 51114. Sampling and Analvtical Procedures All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 51114. Qualitv Assurance All equipment set-up, sampling procedures, sanlple recovery and equipment calibrations \vere carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbook/or Air Pollution lvfeasuren1ent Systems. 7 APPENDIX A: Con1plete Results and San1ple Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Conespondence 8 APPENDIX A Table IV Complete Results, South Yellow Cake Scrubber Table V Con1plete Results, Yellow Cake Dryer Baghouse Table VI Complete Results, Grizzly Baghouse N Olnenclature Sample Equations A TABLE IV COMPLETE RESULTS ENERGY FUELS RESOURCES, BLANDING. UTAH SOUTH YE]J .. O\VCAKF: SCRUBBE:R E::XHAlJST Symbol Description Dimensions Run #1 Run #2 Date 1 1/26-28/1 2 11!28:'13 Filter # 6065 6066 Begin Time Test Began 14:42 10:27 End Time Test Ended 10:l3 ~0:27 Pbm Meter Barometric Pressure * * In. Hg. Abs 24.64 24.70 ~H Orifice Pressure Drop In. H~O 1.255 2.062 Y Meter Calibration Y Factor dimensionless 1.004 1.004 Vm Volume Gas Sampled--Meter Conditions ef 366.358 352.274 Tm Avg Meter Temperature "F 85A 97.8 ..J!:lP Sq Root Velocity Head Root In. H~O 0.7851 0.8106 \Vtwc Weight Water Collected Grams 290.2 278.1 T t Duration of Test Minutes 480 360 C p Pito! Tube Coefficient Dimensionless 0.84 0.84 On Nozzle Diameter Inches 0.2250 0.2505 CO2 Volume % Carbon Dioxide Percent 2.00 i.SO O 2 Volume ~'o Oxygen Percent 18.40 18.40 N2 &CO Volume ,% Nitrogen and Carbon Monoxide Percent 7<.).60 79.80 Vmstd Volume Gas Sampled (Standard) dscf 294.393 278.076 Vw Volume Water Vapor sef 13.683 13.112 B w s (measured) Fraction H20 in Stack Gas (Measured) Fraction 0.044 0.045 Bws (saturated) Fraction H:P in Stack Gas (Saturated) Fraction 0.079 0.080 Bws Fraction H~O in Stack Gas * Fraction 0.044 0.045 Xd Fraction of Dry Gas Fraction 0.956 0.955 Md Molecular WI. Dry Gas lb/lbmol 29.06 29.0::: Ms Molecular WI. Stack Gas lb/lbmol 28.56 28.53 %1 Percent Isokinetic Percent 99,4 t)7.8 Ts A vg Stack Temperature "F 100.2 100.7 As Stack Cross Sectional Area Sq. Ft. 0.887 0.887 Po Stack Static Pressure In. H~O -0.420 -0.420 Pbp Sample Port Barometric Pressure In. Hg. Abs 24.57 24.63 Ps Stack Pressure In. I-Ig. Abs 24.543 24.599 'Qs Stack Gas Volumetric Flow Rate (Sid) dscfm 1.98[:..;..03 2.05E-'-03 Qa Stack Gas Volumetric Flow Rate (Actual) din 2.68E+03 2.77E·~{)3 Vs Velocity orStack Gas fpm 3.0:::E";·03 3,12E>'''03 Curies Radionuclidc$ per sample pCi 10656.5 4946.9 Crad Concentration of Radionuelides pCi/dscf 36.198 17.790 ERrad Emission Rate of Radionuclides pCi/hr 4.304E+06 :::.185E+06 * If the measured moisture content is greater than the saturated moisture level (supersaturated), the saturated moisture value will be used in all calculations (40 CFR 60. Method 4. Section 12.1.7). ** Barometric pressure for run 1 is a time-weighted average (24.6438) for the 3 days testing occurred, SYC Scrubber AVG 100.5 2.01 E+03 2.73E·+-03 3.07£+03 26.994 3.245E+06 Symbol Date Filter # Begin End Pbm L1H Y Vm Tm I/L1P WL.ve Tt Cp On CO2 O 2 N2 &CO Vmstd Vw Bws Xd Md Ms %1 Ts As Po Pbp Ps Qs Qa Vs Curies Crad ERrad TABLE V COMPLETE RESULTS, PM ENERGY FUELS RESOURCES, BLANDING, UTAH YELLOW CAKE DRYER BAGHOUSE Description Dimensions Run#1 Date 5127/11 6067 Time Test Began 8:41 Time Test Ended 12:14 Meter Barometric Pressure In. Hg. Abs 24.70 Orifice Pressure Drop In. H~O 1.589 Meter Calibration Y Factor dimensionless 1.006 Vol time Gas Sampled--Meter Conditions cf 97.336 Avg Meter Temperature "F 83.3 Sq Root Velocity Head Root In. H~O 0.8395 Weight Water Collected Grams 10.0 Duration of Test Minutes 120 Pi tot Tube Coefficient Dimensionless 0.84 Nozzle Diameter Inches 0.2210 Volume °0 Carbon Dioxide Percent 0.00 Volume 0'0 Oxygen Percent 20.90 Volume % Nitrogen and Carbon Monoxide Percent 79.10 Volume Gas Sampled (Standard) dscf 78.932 Volume Water Vapor sef 0.472 Fraction H.;O in Stack Gas Fraction 0.006 Frac!lon of Dry Gas Fraction 0.994 Molecular WI. Dry Gas Ib!lbmol 28.84 Molecular Wt. Stack Gas lbflbmol 28.77 Percent Isokinetic Percent 99.1 Avg Stack Temperature OF 93.1 Stack Cross Sectional Area Sq. Ft. 1.396 Stack Static Pressure In. H:O -1.10 Sample Port Barometric Pressure In. Hg. Abs 24.63 Stack Pressure In. Hg. Ab:; 24.549 Stack Gas Volumetric Flow Rate (Std) dscfin 3.48E+03 Stack Gas Volumetric Flow Rate (Actual) cfm 4.47E+03 VelOCity of Stack Gas fpm 3.20E+03 Radionuclides per sample pCi 6540.7 Concentration of Radionuclides pGdscf 82.8650 Emission Rate of Radionuclides pCi.llr 1.730E+07 Dryer Baghouse Symbol Date Filter # Begin End Pbm ~H Y Vm Tm -V~P Wtwc Tl Cp On CO2 O2 N2 &CO Vmstd Vw Bws Xd Md Ms %1 Ts As Po Pbp Ps Qs Qa Vs Curies Crad ERrad TABLE VI COMPLETE RESULTS, PM ENERGY FUELS RESOURCES, BLANDING, UTAH GRIZZLY BAGHOUSE DescriEtion Dimensions Run #1 Date 11127112 6068 Time Test Began 8:38 Time Test Ended 16:43 Meter Barometric Pressure In. !-Ig. Abs 24.65 Orifice Pressure Drop In. H~O 1.031 Meter Calibration Y Factor dimensionless 0.999 Volume Gas Sampled--Meter Conditions cf 332.974 Avg Meter Temperature "F 80.3 Sq Root Velocity Head Root In. H~O 0.1722 Weight Water Collected Grams 11.3 Duration arTest Minutes 480 Pitot Tube C oefticient Dimensionless 0.84 Nozzle Diameter Inches 0.4425 Volume % Carbon Dioxide Percent 0.00 Volume % Oxygen Percent 20.90 Volume '% Nitrogen and Carbon Monoxide Percent 79.10 Volume Gas Sampled (Standard) dscf 268.636 Volume \Vater Vapor scf 0.533 Fraction H20 in Stack Gas Fraction 0.002 Fraction of Dry Gas Fraction 0.998 Molecular \Vt. Dry Gas Ib/lbmo] 28.84 Molecular Wt. Stack Gas Ib/lbmo] 28.81 Percent Isakinetic Percent 99.2 Avg Stack Temperature "F 62.3 Stack Cross Sectional Area Sq. Ft. 1.917 Stack Static Pressure In !-IzO -0.30 Sample Port Barometric Pressure In. Hg. Abs 24.62 Stack Pressure In. Hg. Abs 24.598 Stack Gas Volumetric Flow Rate (Std) dscfin 1.01 E+03 Stack Gas Volumetric Flow Rate (Actllal) cfin 1.22E+03 Velocity or Stack Gas fpm 6.37E+02 Radionuclides per sample pCi 182.2 COllc<!l1tfation of RadiollucIides pCiidscf 0.6783 Emissioll Rate of RadionucIides pCilllr 4.122E+04 Gnzzly General Nomenclature %1 = percent isokinetic, percent As= (Ds~/4)·1l AS~P = see "tlP Btu = unit heat value (British thermal unit) Bws = fraction of water in stack gas (may have designation of "measured" or "saturated") "measured" represents measured moisture based upon sample volume and water collected "saturated" is a calculated value based upon stack pressure and temperature Co = average of initial and final system zero gas calibration bias checks (ppm, percent) Cavg = average gas concentration (as measured) Ce = concentration of particulate matter, back half (gr/dscf,lbfdscf, etc.) Ccond = concentration of condensibles (grain/dscf) Ccors = concentration of coarse particulate (gr/dscf) CDir = measured concentration of a calibration gas when introduced in direct calibration mode Cfa = concentration of particulate matter, front half, actual stack flow (gr facf) CF = concentration of particulate matter, front half (gr/dscf, Ib/dscf, etc.) Cgas = Cavg corrected for initial and final system bias checks (Equation 7E-5) COl = average of initial and final system upscale gas calibration bias checks (ppm, percent) Cma = actual concentration of upscale calibration gas Cmetal = concentration of metals (ppm, J.lg/fe, etc.) atomic symbol replaces "metal" CO~ = percent carbon dioxide in the stack gas Cp = pitot tube coefficient (0.84) Cp\!IO = concentration of PM IO particulate (gr/dscf) Crad = concentration of radionuclides (pCildscf) CS = measured concentration of a calibration gas when introduced in system calibration mode Cx = Any species symbol may replace X. Units may be expressed as ppm, Ib/dscf. etc. Cx (corr) = actual gas concentration corrected to required percent O2 Curies = Measured radionuclides per sample. Units may be pCi or uCL Dc = jet diameter (cm) DfF = Dioxins and Furans (See laboratory report for DfF descriptions and nomenclacture) tlH = orifice pressure drop (inches H~O) tlH@ = orifice pressure (inches H~O) tlHd = orifice pressure head (inches H20) needed for impactor flow rate Dn = nozzle diameter (inches) ~P = stack flow pressure differential (inches H~O) Dp50 = 50% effective cutoff diameter of particle (cm) Ds = diameter of the stack (feet) EA = percent excess air ERe = emission rate of back half particulate (lbfhr) ERc0nd = emission rate of condensibles (lb/hr) ERcors = emission rate of coarse particulate (Ib/hr) ERr = emission rate of front half particulate (Ib/hr) ERgt/\ = emission rate of a gas (Ib/hr) ERmmBtu = emission rate per mmBtu of fuel ERp\t1o = emission rate of PM 10 particulate (Ib/hr) ERrad = emission rate of radio nuclides (pCilhr) ERx = emission rate of compound which replaces X. Units are usually in Ib/hr. FD = Dry based fuel factor. Ratio of the gas volume of the products of combustion to the heat content See 40 CFR 60, Appendix A, Method 19, Table 19-2 for fuel factor values. Kc = Cunningham slip correction factor A = mean free path of molecules in gas phase (em) mmBtu = miilion Btu General Nomenclature Mcond = mass of condensibles (milligrams) Mcors = mass of coarse particulate (milligrams) Md = molecular weight of stack gas, dry basis (Ib/lb-mol) MF = mass of particulate on filter (mg) tv'tFP = mass of particulate matter on filter and probe (mg) mmBtu = million Btu Mp = mass of particulate matter in probe and front wash (mg) Mp1\lIo = mass of PM 10 particulate (milligrams) Ms = molecular weight of stack gas, wet basis (lb/lbmol) ivlx = mass of species "X". Units may vary and other descriptive subscripts may apply_ ~ls == gas viscosity (poise) M\\x = molecular weight of gas species (g/gmo!) N = number of jets per plate N2 = percent nitrogen in the stack gas O2 == percent oxygen in,the stack gas -Y.6.P = average of the square roots of .6.P (may also be referred to as AS.6.P) -Y.6.P1 == square root of.6.P at point 1 of the current test, Method 201A -Y.6.P I' = square root of .6.P at point I of the previous traverse, Method 20 I A I/.6.P'a\c = average of the square roots of.6.P from the previous traverse, Method 201A Pbm = absolute barometric pressure at the dry gas meter (inches Hg) Pbp = absolute barometric pressure at the sample location (inches Hg) PG = stack static pressure (inches H20) Ps = absolute stack pressure (inches Hg) PStd = absolute pressure at standard conditions (29.92 inches Hg.) 0= time of test (minutes) 81 = sample time (duration in minutes) at first sample point for Method 201A 0n = sample time (duration in minutes) at sample point "n" for Method 20 I A 8lcst"" target test time for Method 201 A (minutes) Qa = stack gas volumetric flow rate (acfm) Qs = stack gas volumetric flow rate (dscfm) Qsc = actual gas flow rate through the cyclone (acfm) Qsce = actual gas flow rate through the impactor (acfm) Q\\" = wet stack gas std. volumetric flow (fe/min, wscfm) R = gas constant (21.85 inches Hg*ft3/(1bmol*R)) Pp = particle density (1 g/cm3) Ps = stack gas density (g/cm3) Tm == stack temperature (F) Ts = stack temperature (F) Tstd = absolute temperature at standard conditions (528°R) Tt = Duration of test run in minutes. Also see 0 tim = mean molecular speed (cm/s) Ym = sample volume (fe) at meter conditions Yms!d = volume standard (dscf), sample volume adjusted to 68°F and 29.92 inches Hg. Y 5 == velocity of stack gas (fpm) Y\\ = volume water vapor (scf) at 68°F and 29.92 inches Hg. Wt\\C = weight of the condensed water collected (grams) Xd:::: fraction of dry gas Y = meter calibration Y -factor (dimensionless) \If = dimensionless inertial impaction parameter, 0.14 General Sample Equations "l %1 = Vmstd· (Ts + 460)· 1039 1(9· Vs" Ps " Xd 0 Dn-) As = (D / I 4) • 1C Bws = Vw I (Vmstd +Vw) CB = MB • 0.01543 I Vmstd Ccond = Mcond 0 0.01543 I V Illstd Ccors = Meors • 0.01543 I Vmstd Cta = Tstd • Cfp • Ps • Xd I [Pstd • (Tm + 460)] Cr = Mfp .. 0.01543 I Vlllstd CPM10 = MpMIO • 0.01543 I Vmstd Crad = Curies/Vmstd Cgas (corr) = Cgas • (20.9 -desired %02) I (20.9 -actual %02) case Dpso = .y [J.lS • \.If 0 N 0 1C • D/ 0 18 I eKc • Pp 0 Qsce • 4)] P~II" Dpso = 0.15625 0 [(Ts ~ 460) 1 (Ms 0 P s)f2091 0 (~ts I Qsc)O.7091 ERcond = Ccond • Qs • 0.00857 ERcors = Ccars 0 Qs • 0.00857 ERF = Cr· Qs 0 0.00857 6 ERgas = Pstd • Qs • Mwgas • Cgas • 601 (R • Tstd • 10 ) ERgas = Cgas(lb.!dset) • Qs .. 60 (Either ERgas equation gives equivalent Ib/hr values to 3 sig. figures) ERmmBtu = Cgas(lb:dset) • F d • (20.9/(20.9 -%02), Method 19 Equation 19-I ERpMIO = CPMJO • Qs • 0.00857 ERrad = Crad • Qs • 60 Ke = 1 + 2 • I\, • 1.257 I Dpso I\, = p.s I (0.499 • Ps • U m) Md = CO2 • 0.44 + O2 0 0.32 + N2 00.28 Ms = (Md • Xd) + (1 8 • Bws) ~ls = [51.05 + 0.207 • (Ts + 460) + 3.24 -10-5 • (Ts + 460)2 + 0.53147 • %02 -74.143 • Bws] -10-6 Ps = Pbp + (PG I 13.6) 91 = (.y~PI' I .y~pla\e) 0 (9test I pts) 9n = 9 1 • .y~Pn/ ..J~PI Qa = Vs· As Qs = Qa • Xd • Ps • Tstd I [(Ts + 460) • Pstd] Qsc = [(Ts + 460)· Pstd I (Tstd • Ps)] 0 [(Vmstd + Vw) 19] Qsce = [(Ts + 460) • PStd I (Tstd • Ps)] • [(Vmstd + Vw) I 9] Qw = QsI Xd Ps = Ps 0 rv1s 0 3386.39· 10-6 1 [R .. (Ts + 460) 1 1.8] Zlm = 100·.y {[R· (Ts + 460) I 1.8· 8· 103 ] / [n· Ms]} Vmstd = Vm • Y • Tstd • (Pbm + ~H I 13.6) I [Pstd • (Tm + 460)] Vs = 85.49 • 60 • Cp • .y~P • .y [(Ts + 460) I (Ps • Ms)] Vw = Wtwc • 0.04715 Xd = 1 -Bws APPENDIXB South Yellow Cake Scrubber Prelin1inary Velocity Traverse and Sampling Point Location Data Field Data Sheet Yellow Cake Dryer Baghouse Prelin1inary Velocity Traverse and Sampling Point Location Data Field Field Data Grizzly Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Field Field Data B South Yellow Cake Dryer Scrubber Prelim 8 pts blank Facility Energy Fuels Resources, Blanding, UT Stack Identification South Yellow Cake Scrubber Date L/~)C...--/ i-. i Barometric Pressure 8 Pbm 2:..~(/?--in Hg Pbp l. '/. "'/ j-in Hg N AO Static Pressure (PG) -, tf l-in H2O Estimated Moisture (8ws) .J -t.. G7 % Sample Height from Ground ; , := ZO feet Comments: Stack Dia. 12.75 Reference: 0 Ports are 7' Upstream from next disturbance Ports are 30' DO\\-11stream from last disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B C D E F 1 6.7 0.85 0.85 ~~. fJ.5-1 2. 2 25.0 3.]9 3.19 '1..t:, J 1/ 3 75.0 9.56 9.56 /C// !Jb '/", , ~ 4 93.3 J 1.90 11.90 1"1:,11 't /I-J , U- Averages: Ts L. Flow ---- j,p '-illP -------- KEY => I ..... T_s ___ ll_P_L._F_IO_v--,vl 2f :t: :-! .. -..."., ~~~~ ,~~ '\':1' :.7; < 0.. < - g S:\o ::; ~~. ~. g Z :.r. :.7: f'., .. :~ ~\ ~ \ .... \, ~,~ ~ \ .. <~ :-~ OJ £ - \ ~ \.~ > -'" ·~.I ~I \,,".";' I ~\ /,/ c J held I )al;1 Sh~l'l Plunt: Ener!!)' Fuels Rcsoun:t:s, Blilndin~. l JT j)atl~: / /,.,' ,5 . Time 'I l)(if\l I~ /\H (,nlt.Oj ~'j(lck I Min (Il) I. CUi. • (," II I), Desired Actual Trawr~ ... 1'01111 ~~' 97, 'Il7J I/P ,/ ./ (i..:?/ / (,' " I /'? ,7 1 0 ( t, .' -" , " /J~ 1 1 (,r-7/l 'l "/ () --'-';'~ (, ), j.' 7 :) ~, " F·{'.L V"~IIU1l1 huH;' (..-/ L./ 'IFrco hll~'1 (., [-:'{; b' Salllpk Ho" (,; c..J :~), ", ,/J"':'~" l.ocation, South Ydlowcah' Dryer Sl'rllbbl'r ( )p~l'attlr: ;, ,') (~'/J (" Tcmpcratlll'cs ,"1. " DGl\l Temp ('1' ... ) Slack ('1',) I ProhL' I l'whdlul I Filler I EflhlL'llt" Out In 4 "".,"n I.", / .' I L) --;1-;,)'--1(./ 1 ';---1 II t£; ':I 1 r...) ,7 (, r.~.t "t," l j Jol' ~" ,r L....:. . ,., ," j .J' .., •• I i:,,~; 0 / .I )"/], I). c.: f· 1/ (;;-)", '-/7 cB ~.r ;7 i I'agt' ' \.(' Rlln :; B r AO N Stack [)iamc!~r 12,75" )lort Reference O,()" 1 ) (~ /7.;;:. 0!J { . /,~ ',:' }, '/1./ /./ (~ ,; ,/. / / ,f,,' (,. • /,'" '0'" '} ," , )' '--, ii~ .<.' '-' /-, ., 1/1(/.7 )'/0').7. /',r. / "" ./ Ij'\ k' / /.., Ports arl' 7 I JpSll'l':t1ll I rolll Ilt..':>;t dlsturh:l!l(:l' l'f .l' ,Ili/,) j /, I Ii :7 il,/C' ,/, /e' .,,)' I 7 ~-) -)---t ' )"/( 2 , -', .' 1" "I ," \---/ c;:: r L~; ~/' / C::{" )/7. /. 7 I ).t.~, V ./ ~ {,. () -LL Ports are 30' ()owllslf'l:alll emmins! dislllrbance , /:., , (/,' ~ ,-. ~ '--/ (, 7'" .;.". (; (: '{:~ 7 /,.1[' ""r >. j , • )./ i)" 117 h <f '3 U rfc71rBT .I.1l' l!.(.:"t/~ ,~ ;' '{",'- -:11 'II ' I' Ip.::--j / l { ). '( L"", .Nt', / /,J ~ ,) ,~~_ t..~,'. 7(~'~ AsslIlllcd MllistllJ'e 5-13 "i, Z<c:L 21/ ' ).6 / 2/'/ j'/, t, 7,,: ~/ "f ) .j 1)(. '" ( .. , ((),7 :.:'" '1(:' 78(..;, (j) ('(' ,7L/ ),)). )".),7 , 2 / .'}U 3 / .:.::':'f I ;c y -3 ., "6' ,,'" .' II 'II ' '-I "II' 7 II ' .I /('')''11 Ol--c', / i/ 17'S ~,,-/,,:/). ',/.' If / / {;" L/ .2 : (/'C' 3 /1 en' II ) I.)'~ (./ ({. 11/ -7) II) ',), c/l).-.)·'l/ll':; II {i q I'}-J 71;.;)-0 1):/-) .. \ 6' / II {::! / Ii />/_~r /' ,'1,1'-4 4 1.-.' ) (~:.' J -' '(I'-4 /t~ f" ~to\ .1{}1-. ~~ 1.. ~"L. t. -J, -V 2/ C1& 'l.t~c:r t~ ~:'D s J t1'L II n ') ~ (/t./ 16(,.' v1-':}-· IS-V ,iP"~-"---'-- ,J .-(,;(./ n 1 ['3:,) Iff () <o1~~ lo"L--(o~ 'L'() \ "2-~ ~. 1 <{ 711J~ zt,,\ 2,., C s-=t-IS-J D3 ? ./,r 1 1(/)"· <6'"<1 lr ¥l~ -.. til 'l.01 2-,6* '''1. 2. hi. 2HO 2c.(1) l-{ &; Cit/} ~~ ;7,')(.' 1 l(e) 0] O~1..4~C ·foe: 1.·0\.-j 'l.O~ 11+ 4~ 'l{p""+ 't-(o~+. "'L-~C L.j (0 '1<;" loy ):l(/'-2 /1;-' ~Z.1 .... ~(Pt1 ~(P"U' "~Y 1.()1~ L:.-IDO 7(oY 11#(:;---z.(;c;-~ t Ci''1 fOY t-Ifc't· 2 !~ll(t ~"){P.11,,~~~(p~ l·t\1-\''17 ,.. 0f 10\i(P) 1,,::}:7' t-::}D Llf ot3 JDj- "f <1/-2 }):r-q ~\ ,ttib ~ (; J. Vj (.4 ,~l b~ /LvJ'1 "2. 1-'1 1-rfc '1}5 I,; lOb vll)t:: 3 ).70' q(P5'.\$'~t·ft, 1·'1 I-Ll: 0/ Io~ "l.('$ '1.,"" 7..V1 50 C(3 to f/l.'vl)-' 3 ? ... 8'F" 0]~-4.~'~~ . ~ '0 t·q~ \. '\--1 c: 1 '0:;' '2 ~ "'2-'-1 D -z, l( Lf5 '13 /bS" J-:'i/{/ 3 j~O{) qq ~ '(J?4t _ (p I l·q I ( .q (01 0) 1-c,(p trl.::}\ 1/~ \ Y:V '1~ I b~ ~F-:lf-4 ) II-'-I 001'". 1--J..~' . (0.> ,." :}" \ ·Q"1 /4-J '01/ 1Jt;"\ '1.. 1-C 1 ... '1:l C\ .... + q ~ I bra ,"-:;>{) 4 ?}() IO~'l--·\1.1lv ,(,('-,,(.-V ~. «~/ fII".:r 1'(;1.0 1..,VL,1.:"\:\ "Z;(f ~<{ 1?:> InC( f2 {()--4 )Lt;--I b ~1.tJ .t4V-1 .lD'O ·W I·W 4 'DC; 1A(}v 'U tL t 1--\ tf'1 C1 '3 I c><6 (; .'f/(/ 1t,:;5 '3 {~(~ I ot;O .tp'U -. '~1~%'111:i~~ ~ tq·~5~~~~.(tl'/ ~~lt~' ~~ .--"357.' 'Z --:r-.J ~ f; l olo /l .r.}.!J t.·· I Db' t Total AVL'rage Additional (Extra) Leak Check Information DGM before Leak Check Vac ("Hg) Rate (fe/min) DGM After Leak Check <6'f1-'/f:>f( \ \ l5 ~()D5'" 15~Y.IOv 4&1,5- Cj 1-C;;' Vac ("Hg) \ \ .Prohe /: /' /r Cp 0.84 Nonlc Calibration . ,Z /7. .. ~ (if? ;) :,-/ :..2ZL Avg DII ,)}"( .. / inches (ias nag //'::>-j. Console I"f Y-hlct(lJ' ,I, ( ,:~ f\H@ / I ~/ '~I ('i'll liP B:lnlllletric Pressures Phll.,/~·'1·1 r;'~__ in JIg Phi' ·?~,Y,(lL2 .. _. in Jig 1'. . -i (./? inll,{) if, ':/7 ,~,>-/.q'-/J' ',-'. .. I,~ak fhed, e.n~ EQ;5I n'':nllll ,t:·;;·· '? V:It"1I Ilg j~!, / 1'11011(011,' {-: l- In'I)O I': ( C£ '\ Watci Cl>lIccl~'d 11'1 g Rate (fe/min) '(};l)t)~ T;",< Sampl«1 ~. { m;" l{t'\IC\\' K K 111''1'", :a'T", Yellow Cake Dryer Baghouse Prelim 6 pts blank Facility Energy Fuels Resources, Blandjng~ UT Stack Identification North Yellow Cake Dryer Baghouse Date 1 Barometric Pressure B Pbm in Hg Pbp in Hg N Static Pressure (P G) in H2O A Estimated Moisture (Bws) 1 % Sample Height from Ground feet Comments: Stack Dia. 16 Reference: 0 Ports are 57" Upstream from next disturbance Ports are 468" Downstream from last disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B C D E F I 4.4 0.70 0.70 2 14.6 2.34 2.34 '(J?.; {,.j 3 29.6 4.74 4.74 4 70.4 11.26 11.26 -or .~ y . ~\ 5 85.4 13.66 13.66 6 95.6 15.30 15.30 ~Y' "l'tl Averages: Ts L. Flow -------- ~p ,j~P -------- KEY=> ttY v\~ ,~ Field Dnla Sheet Date: _-" ' , Time Tr:lvc,s~ II-I ----.--:-:--:::-:1 1'01111 II CI\lt~k I Min (0) ):'-(1 o 2 to 3 '(U 4 ·~D 5 '1° 6 )'1) 0-·\4 {jO 2 \ 7.0 ' 3 15'U 4 --'i j) 5 iuJ 6 Itt) i(A) Total i\ ('Ollllll<:nb Time r-~:\.l\ S ~~ 1~Oc t..-1f ~: 3-c to" ot DOM W'l (~s. .'3., 10 ~ (p (,1_ .. l-B b(t''!. ltJ--l ~r}-q ~'j( (, \r /F JOt> ~~b\ -'}O:{ . .I -H (p -tU .. -rtl ~-r\ (~ . "7 y{ -j-~~~-~ 1.-~~1:i:J I 14[.,-:rrV ~o .... \;tJ bUb :1FE'rco. ;5 Filler, . ' ? Sample Box Location: North YeIlo\vcake Dryer Bughouse .... ) Operator: (/'''/'---'1 ,\P L\H (,"HPJ II V"~lUlI\l11 Temperatures 1''1') DOt,,1 Temp ('1'111) ill ",.If,II, II Desired I i\t~tual II I'" If,' II Slack (TJ I Probe I I'roh~ (lUI I Filter I Effluent II Out In v'(t-. --;~)ip (_.LQ~ ~ '-\ 1..\ \ ~ , D ~ \\\~ ~~~\ \q~(6 ~ 'Co ~~ ,-\' <;~ "'\ '5')' 3> BaghouseAP Time BaghollseAP ./ {O', 3D ,-;//(J L:1 ......-t I: 00 if· :;-7 , ? ,"\ :~~ t.("~--(\ \1-',00 ';.0 ! r)'. L-,', n q Page.: ( 01'.\ Run if I B r AQ N Stack Diameter 16" Port Reference 0.0" Ports arc Ports arc 57" Up$(r~~am from next disturbance 468" Downstream from last disturbance Assumed Moisture ~'o Probe If -t~, ___ Cp 0.84 Nozzle Calibration ~~ • 2. Z( • 22.-·( • 2-& J AvgDII .22·l inches Gas Bag Ambient Air Console ~ J Y-Factor~ t.\H@ 1'(1'-( in H~O Barometric Pressures Leak (,h~ck; fr'fmin vac in Jig Ph", --;Z':L~t%-__ ---in Jig PhJ1_~z::'j_(_~ _____ in I-Ig P(L, ___ =-J.:J ... ________ in H20 Pre D.6lJt- L2 Post ' 0: DD t/-rz-\ ().b /") -PiloIR:lle~ ~-.... --InJI~O~ Water Collected (C-,(l. Q ~---g Time-Sampled' ( 2/q min '\i"" r~eriew" (-'''\. K ~, K @T," (tirl' ,-. Grizzly Baghouse Prelim 12 pts blank Facility Get1isen-Mine.s e", t' /11; t F<./~ I /,Z')"' /, .., / Stack Identification Grizzly Baghouse Date ----------------- Barometric Pressure Pbm in Hg ----Pbp in Hg ---- Static Pressure (Pa) in H20 Estimated Moisture (Bws) 1 % Sample Height from Ground feet ---- Comments: --------------------------------------- Stack Dia. 18.75 Reference: 3.0 Must use 3611 probe or longer to keep box o1,.ltside .handrail __ _ Ports are 24.5" Upstream from next disturbance Ports are 4811 DO\\TIstream from last disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B c D E F 1 2.1 0.50 3.50 2 6.7 1.26 4.26 " 11.8 2.21 5.21 -' 4 17.7 " "') ..) . ..) .... 6.32 5 25.0 4.69 7.69 6 35.6 6.68 9.68 'i1,; , c 5,::· 7 64.4 12.08 15.08 8 75.0 14.06 17.06 9 82.3 15.43 18.43 10 88.2 16.54 19.54 11 93.2 17.48 20.48 12 97.9 18.25 21.25 Averages: Ts LFlow --------- ilP ~~p ---------- KEY=> hdd Data Shc(:t .... JT~TCO Filt(:r ~ q:~_l? Sample r3o"\ Plant. Berttson-Pv'ltnes [3'1 "";,,, k -c ;-'""'v v 4 "j ,,_ J / Date: jlrl, II ~.., 1i~.,.I·, l.llcHtion. Grizzly Bnghollsc Operator: i"Y\, t.A..! 'l~\ t .. ,J !;,\'A lr/d', rr~lV':!':.c Time nOM i\P L\H (on 1'1,0) Va~uwn Telllperaturc~ (I, 1'('1111 Clock Min (O) I JI ~ Im!t:1h Desired Actual !mil;.') Stack (TJ Probe I'rub~OlJl Filler Efllllcnt () 1 B::>,'t 0 90o,oo'L .0 lJ ,g<i , ~o (-(..\1-2.1\.. z. ·,{o I (0 5'-t 2 7j'" /0 '-1 n. {.oZ';-• O"3l: ~ .(,L. I..() l,. L --19 l'-iz.. (, -r""" l <..f~" 5"-1 3 '10 <-tZ-';-, '10 • ()Ji) I·Cz..,. l.()[.. 1.-50 L3t.t z.-( j 'l. '-J-5' 5~ 4 LO 'i3~\·~'O; , o'~~ 1,,0'2,-Lol..-l-~L .. Vo'8 '1.\0'0 lfQ ~2. 5 80 15:5. :)OJ .'0 :3:3 \-1'-\ \,l'-{ L. 5 ') l3l tbO (.'-)9 ~{ 6 to<'; ~~?>,O)( '03{ \.1.1.-1.1,?", S St.l l.-J~ l...ro l..4Q lot 7 n.\) \..1 R z... 8LQ i 031 l .0'S t.o~ 3 sc 'l)i L{) ll.{3 ~3 8 \'"'\0 99' l."(.{' • 'i:t,'L. j, • It 1.\1 ~ 5R l.,r; -:::{-l'{~ l.'iO b'O 9 11.,'1) io\\'L-\?>f' .03\ I '0<0 l.oB '3 (p/ L ')( l{q z,<'/'o ~o 10 180 j 0 l.5 ,'-\30 • 0'2.71 ,q,-\ • 'i t\. "J ,) (,) z. '-r::r Z,{L\ l'f) "or 11 loO 103$\, D'1D 'Ql.~\ t. 0 i 1.0 t 3 {,(, l,)~() lS) LY~ 65 12 11. \38 l.1.0 lD5L.'1rS/ • 0 I..-J.. ~ '1'1 j '( <i 2-~9 2;J l~O 1.. ... /9 5, J\ 1 ~ ~~ I. t{, ~ ll..\<> \ 0 (,(;" lo( BI;, J ~) '1. ~/~ , '-f() , (.·t iJ L,· ( ~t '-' ; ~7""; £.)'0( Z. /" 2· v( 2 l6Q 10 'let (t-'" • C:.1l. 'l . '"'Itt • '141 L, ~i 1..::5'0 l"'l) Z'io S3 3 L,~o 1092.Cl:to • 0 7..:/ .t;n .. • 'ri"1-t.-'10 l.00 ~t.tC( l..(.H 5'-{ 4 30'0 \105.161-) .oL~ ,40 • ''10 2.-10 L<.,o L~q l. ... \ y' 5,5 5 ~LD Ilj<t.~ .. \{ 'U~O Lo<-t t· oY. L 70 l'a (' LLj{/ L<-to S9 6 4~0 1 t")") . >(.,0 ot>'YL ~ . It t. \ \ z.,. 70 LG:,L.. 2.ri-l~8 s'q 7 )(.,0 , I '{ "l-. 'i 1.5' .0 OJ! ,.00 !.oq L. -1 \ 1..70 lIt l(,)' ~o 8 3Wo \ i(.. t. S:)0 • <'1"\ j. D~ \,Oe 1-II (,{ r 7. GO ~:,~ "I 9 l..loo lnS.501 ·oY> totl lot( L ,f.., ~j-i10 L7J 2.<.> r ~o 10 i--IZ,O I I e\i) . ("(00 • t)'\ '") I ,t·)''' J. t{ t. (, ~ (.<{l; l.'io LeU 5C( 11 1.( ~tl!j) (lD1. ilct{ ·0 l.'i t·o! l.-ol L \,,) l~~ Lc..tB l'ic..{ 5(, 12 Lf<.,u 1 l. I 0 ~=fJ.,:: '030 i,O'-1 \.04 1.. ('Ii...-L1.t.{ Ll{) L39 .),) If., >L!> '-t~iO 1'~ ')!. .'-flL, Total 1. ,7 / 0'1 , ... ,;. "1 r ,) J -. I j 'y _'-::L!2 L (~~ Lq .... -l'-'[u ,'--l<-jL, Average v • t "7 (2/ l.O!J i IvL. ~ (~(\lImh~l1t ... DGt.,,1 Temp (Tn; l Oul In <-t C( 48 :5L. (uV 59 ('q () ':.}-78 -1 J 3i i'f) 8't 9t't_ en 8~ 9<0 l6'l' ~C B(r., Lf l'..f 0./ 0) '12.- ~) 1e... t,L; 1.>. r t,..)\ 7-7 a.:> 10 B'-t 7'{ g( 7'0 13ti 7~ 3 -7 "r- 31. ~0 'Ot y)g 81 99 rao g'·:r 78 8\9 '1 b \j) 2 () c,.' ''1 J 0,..1 J ~[) .-~ Page or J.. Run Ii j r AO" N Stack Diamcter_,. 18.75" Port Reference _ ... 3.0" _ Ports are Ports are ~ Upstream flOm next dIsturbance 48" Downstream from last disturbance Assumed Moisture ____ ~'O Probe ~)i-17 Cp_ 0,84 Nozzlt: Calibration . 'til.. ''-{41 .L{L{:;' 't1\.{ "3 Avg 0" "".15U;· inches Gas Bag Ambient Air Console __ l...:...lJ __ Y -Factor ·cref 1 L\H@ L -Lift J in H20 Barometric Pressures Pb," __ ._:~':L:_,~ r _____ in fig PhI' _. __ ._~.'"l,', \?,:._~ ____ , in Hg in H~O L<!ak Check l:E Post ft'/1l1111 [1 .,' /) (, O.O() l· v,le 1IIIIg l C1 ~ Pllm Rah! 0.1.1 J ,IJ In H:O I IQ • '7..0 Water Collected ,j! ' :') g Time Samplt:d {1 WO min Review JJ(~\li,. K ,~ K= @Tm @T", South Yellow Cake Scrubber Sample Recovery Gas Analysis Data (ORSAT) Yellow Cake Dryer Baghouse San1ple Recovery Gas Analysis Data (An1bient) Grizzly Baghouse Sample Recovery Gas Analysis Data (An1bient) Chain of Custody Lab Analysis APPENDIXC c South Yellow Cake Dryer Scrubber SYC Date: Facility: g~n-M1neS' !3J4 C7~~r I-~ t:!d Stack Identification: SYC Scrubber ---------- ------------------------------------ IMPINGERS Filter Number: ~b" ..,;- Final (g) Initial (g) Net (g) IMPINGERS Filter Number: (ij tt: IMPINGERS Filter Number: Final (g) Initial (g) Net (g) Final (g) Initial (g) Net (g) Run: i Sample Box: /J Implnger 1'lumber 1 2 I 3 I 4 I 5 6 Initial Volume of liquid (H20) in impingers, (ml) drop out 100 I drop out I 100 I MT SO I 3 6tJ/t J °77diJ '1'fI',.Cj 7/J-: 'i ~/6r/ 'j'Cl..2.,O 5s).~ ~f{·e '17>,5 L.C(2, \ ~01· w~ ell,L.. (,/7,7 ,I )"] r-;2). I {..f ).],p:: 8~J--l ~', .c~ I 0·'-"'".. I'~' ~.i ~> c";, Total (g) ",'-' / ========= ,., f ~';;~~.,i Run: L -~--Sample Box: l:: ---- Impinger Number 1 2 I 3 I 4 I 5 6 Initial Volume ofliquid (H20) in impingers, (ml) drop out 100 I drop out I 100 I MT so t,c.-f1-:3 +3s: c) ~S-1·6 t,'1~. 0 533·0 cr Lj~. ('" .> -6l-~J -£§t% 'I LJ V 7/; , ') /.' ") J-:J :.:, I t7 9,7.' f') I r I # ,-.I C:,.. \/') I. / &G~~ 1-<1--4 L? l.'-[; 11..1,., u.. s-/--r,?'y-' :J /, Total (g) ======== Run: ----Sample Box: ---- lmpinger Number 1 2 I 3 I 4 I 5 6 = Initial Volume ofliquid (H20) in impingers, (ml) drop out 100 I drop out I 100 I MT so -------+-------r-----~-----+_------~------ ------~------_+------~------~------r_------ ============================================== Total (g) ========= //)£;7-~ Plant !3:t. "£-'/' '":; ~ ~ (r Analytical Method ORSA T Date /11;~?l;{) i / Test No. Gas Bag No. /+C--j. Ambient Temp ? c CJ Operator .//t£ Date ) j.---).Z~!2... Test No. A Gas Bag No. ----e0:r .. / ...... C..:;.,.<_-=1."'--_ Ambient Temp __ 7'---11:v;...?-r-'l'_ O 1.4.' Ai perator v .// r, __ .c.-4'-~ Date -----Test No. -----Gas Bag No. -----Ambient Temp ____ _ Operator ----- Gas CO2 O2 (Net is Actual O2 Gas Reading Minus Actual CO2 Reading). N2 (Net is 100 Minus Actual O2 Reading). Gas O2 (Net is Actual O2 Reading Minus Actual CO2 Reading). N2 (Net is 100 I'vlinus Actual O2 Reading). Actual Reading ). /:; ,v ) 0 "I Actual Reading ! g Actual Reading Location __ .J---:..Y_·_?_...::!J:..-..:.~...:-/'_?....e· '~,.,,;z:../'--':'C-:::; .. ~7 /:!:..--____ _ Net ).~ /$. 'I Net j, (] Net Actual Reading "l~d }p .. L/ Actual Reading ;, g Actual Reading Net ,J r' .,,<.,...../ ($'1 Net /: 0 Net Actual Reading ~ ~L';:,.I .J-v-y Actual Reading It g Actual Reading Net ';_..,..c;;/ /:%' .. v Kef ~ c' . t z:J Ket Average Net Volume ,).. ... C,Z:./ /df,y Average Net Volume /8 Average Net Volume co is not measured, as it has the same molecular weight as Nz Yellow Cake Dryer Baghouse Dryer Baghouse Date: //-,).,g--2 Stack Identification: Yellow Cake Dryer Baghouse IMPINGERS Filter Number: ~o~'1- IMPINGERS Filter Number: IMPINGERS Filter Number: Final (g) Initial (g) Net (g) Run: J -----:.-- lmplnger Number Sample Box: ---;..,9~· ~_ 2 I 3 I 4 I 5 6 Initial Volume of liquid (H20) in impingers, (ml) 100 100 I I so I ~77' 'f 7' '1 '1,.1-~ / fj, i-9f)./ "'l'Ol'1-(;-oe.1-L{\..t· \ ~lk(:=t- .... ,PJ; ~ J:O ttl / )J;cf Total (g) l?J~ 0 ========== Run: ----Sample Box: ___ _ implnger Number 1 2 I 3 I 4 I 5 6. Initial Volume of liquid (H20) in impingers, (mI) I 00 100 I I so I Final (g) -----I------f----+----t-----t----- Initial (g)-----I-----I-----+----t-----t----- Net (g) ======~================================== Total (g) ======== Run: ----Sample Box: ___ _ Implnger Number 1 2 I 3 I 4--I 5 6 Initial Volume of liquid (H20) in impingers, (m!) 100 100 I I so I Final (g)-----I'-----4----+----+-----t----- Initial (g) -----I----4----+----+-----t----- Net (g) ====:::l===::=!====:!::=====:!::========= Total (g) ======== Grizzly Baghouse Dryer Baghouse Date: Stack Identification: Yellow Cake Dryer Bagh-6use-- IMPINGERS Run: ---.::.----Sample Box: _-=--__ Filter Number: (~ C (, t:' !mpinger Number .A. I 3 I ...i-I 5 6 Initial Volume of liquid (H20) in impingers, (m!) 100 100 I I SG I Final (g) !J ~ --{ iQ ,) j \.{ 5 7J " '-{ q s ~ ,,) ~----~r-~--~~~-~~~~--~-----~------- Initial (g) _""_" "-=; .,~;)~. :.:... ... ~'~_.j_' ...;;,.~;_.--l_, _)' -+...;:;j::.,.. . ...;;,.5_'_1_, '-t~:-+-"(..t....1 "'....".( ~B_. :..or;;"..; ~ _____ ~ ___ __ Net(g) .... ,'J;(.., 2.l~:S ~\15 ::>1·:::;-========================================== Total (g) ======== IMPINGERS Filter Number: IMPINGERS Filter Number: Run: ----Sample Box: ---- lmpinger Number 1 .A. I 3 I 4 I 5 6 Initial Volume of liquid (H20) in impingers, (ml) 100 100 I I SG I Final (g) ----4-----+------+-----+-----+----- Initial (g)----4----+-----+-----+-----+---- Net (g) =======6======b=============b============= Total (g) ======== ---------------_._-_._--_.---_ .. _-_ .. _--.. _-_._.-.-... _._ .. _ ..... Run: ----Sample Box: ___ _ lmpinger Number .A. I 3 I ...i-I 5 6 Initial Volume of liquid (H20) in impingers, (ml) 1 00 1 00 I I SG I Final (g)----+----+------I-----i-----+---- Initial (g)----+----+-----I-----i-----+---- Net (g)===~====='=====::!::===::::!::::========= Total (g) ======== ~~ .:. .'t ~.~,: ~>~:' :; ;.:~.,~ .~;~.;;~~~.(.:~;\~I.~.;~ ... ~.~,:.)~ ~.i:;,r Chain of Custody Record· TAL-4124 (1007) Client Tetco Address 391 East 620 South City I State I Zio Code American Fork Ut . 84003 PrQi~ct Nam~ and l.ocation (State) : Denison Mine 2012 4th Quarter ContractlPurchase Order/Quote No. ., Sample 1.0. No. and Description Date (Contain~rs for each sample may be combined on one line) R 1 Baghouse filter (6067) and beaker 111/27/12 : R 1 SYC filter (6065) and beaker 11/26-28/12 R 2 SYC filters (6066,6075) and beaker 11/28/12 R 1 Grizzly filter (6068) and beaker 11/27/12 Temperature on Receipt __ _ TestAmerica Drinking Water? Yes 0 . No 0 THE LEADER IN ENVIRONMENTAL TESTING Pro/eet Mana,qer Date Chain of Custody Number Dean Kitchen 11/30/2012 TeJepllona Number (Area Code)/Fax Number Lab Number J I 801-492-9106 Page i of I Site Contact I Lab Contact Analysis (Attach list if Scott Christensen, Garren Palmer more space is needed) CaflierlWayblll Number Special Instructions/ Containers & 0 Conditions of Receipt Matrix Preservatives 0 \D ri .... ffl N <'l' lIS N <'l' -c ~ ~ g 5 ~:t: Z ± lIS ~ :::, lIS Time ~ ~ ~~ l-e;: C1I .~ :a § ~ ~ ~ .... -q; ~ C/) C/) :J: "l~ 8:00 X XX X .X! 8:00 X X X X, .. X 8:00 X X )( X X: 8:00 X X )< PossIble Haz8rd Identification I Sample Disposal (A fee may be assessed if samples are retained o Non-Hazard o Flammable o Skin Irritant o PoisonS o Unknown 0 Return To Client l2ko/sposal By Lab o Archive For ___ Months 3. Relinquis/led By Comments o 14 Days 0 21 Days 0 Other' as per method Time r 1/ ( When Complete Email to:DeanorPaultetco@tetco-ut.com DISTRIBUTION: WHITE -Retume7f7075lienl wilh Report; CANARY -Stays wilh the Sample; PINK· Field Copy longer than 1 month) Q~ Roquirements (Specify) 1. Received By Time 2. Received By 3. Received By SDGKo. Order No. 46099 TestAmerica l'ptSTLRchTitle v3.73 TcSlAmerica Laboratories. Inc. Analytical Data Pacl{age Prepared For Denison Mines (USA) Corp. Radiochemical Analysis By TestAmerica j 2800 G. W. Way, .Richland fVa, 99354, (509)-375-3131. .J Assigned Laboratory Code: Data Package Contains 17 Pages Report No.: 54130 Results in this report relate only to the sample(s) analyzed. Client Sample ID (List Order) Lot..sa No. ,\-Vork Order Report DB ID Batch :'io. R 1 BAGHOUSE FILTER J2L040424~1 MXGQT1AD 9MXGQT10 2340042 (6067) AND R 1 BAGHOUSE FIL TER J2L040424-1 MXGQT1AC 9MXGQT10 2340043 (6067) AND R 1 BAGHOUSE FIL TER J2L040424-1 MXGQT2AA 9MXGQT20 2340044 (6067) AND R 1 BAGHOUSE FIL TER J2L040424·1 MXGQT1AE 9MXGQT10 2340045 (6067) AND R 1 GRIZZL Y FILTER J2L040424 .. 4 MXGQX1AA 9MXGQX10 2340044 (6068) AND R 1 GRIZZL Y FILTER J2L040424-4 MXGQX1AC 9MXGQX10 2340045 {6068} AND R 1 SYC FILTER (6065) J2L040424"2 MXGQV1AD 9MXGQV10 2340042 AND BEAK R 1 SYC FIL TER (6065) J2L040424·2 MXGQV1AC 9MXGQV10 2340043 AND BEAK R 1 SYC FILTER (6065) J2L040424 .. 2 MXGQV1AA 9MXGQV10 2340044 AND BEAK R 1 SYC FIL TER (6065) J2L040424-2 MXGQV1AE 9MXGQV10 2340045 AND BEAK R 2 SYC FILTERS J2L040424-3 MXGQW1AD 9MXGQW10 2340042 (6066,6075) AN R 2 SYC FILTERS J2L040424-3 MXGQW1AC 9MXGQW10 2340043 (6066,6075) AN R 2 SYC FILTERS J2L040424-3 MXGQW1AA 9MXGQW10 2340044 (6066,6075) AN R2 SYC FIL TERS J2L040424-3 MXGQW1AE 9MXGQW10 2340045 (6066,6075) AN ----_._ ...... --._._--------_.-...... _ .. --------_ ... -.. -... -.. ~.-.. -. TestAmerica 2 THE LEADER IN ENViRONMENTAL TESTING Certificate of .A.nalysis Decelnber 31, 2012 Denison lv1ines (USA) Corp 1050 17th Street, Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab Project Name Sample Type SDGNumber I. Introduction December 4,2012 Denison iYIine 2012 4th Quarter Four (4) Stack Filter Samples 46099 CASE NARRATIVE On December 4,2012, four stack filter samples were received at TestAmerica's Richland labora~ory for radiochemical analysis. Upon receipt, the samples were assigned the TestAnlerica identification nunibers as described on the cover page of the Analytical Data Package report form. The samp1es were assigned to Lot Numbers J2L040424. II. Samplc Receipt The samples were received in good condition and no anomalies were noted during check-in. 111. Analytical Resultsi.Ylcthodology The analytical results for this report are presented by laboratory sample ID. Each set of data includes sample identification information; ~nalytical results and the appropriate associated statistical uncertainties. The analysis requested was: TestAmerica Laboratories. Inc. Alpha Spectroscopy Thoriwu-228, -230, -232 by method RL-ALP-OOl Uranium-234, -235, -238 by method RL-ALP-004 Gas Proportional Counting Pb-210 by method RL-ALP -011 Alpha Scintillation Radium-226 by method RL-RA-OOI 2 Denison ~/fines (USA) Corp December 31: 2012 IV. Quality Control The analytical result for each analysis perfonned includes a minil11U1n of one laboratory control sample (LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Connnents" section. V. ComnlCnts Alpha Spectroscopy Thorium-228, 230. 232 Sample R 1 BAGHOUSE, the blank and LCS were recounted due to high tracer yields. The recount on the sample and blaILle are within limits. The LCS is slightly elevated at 121 %. The data is accepted. Except as noted: the LCS, batch blank and sample results are within acceptance linlits. Uranium-234, 235, 238 The achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to historical process lalOwledge. The sample activities exceed the 11DAs. Data is accepted. Except as noted, the LCS, batch blank and sample results are within acceptance limits. Gas Proportional Counting Pb-?lO The achieved NIDA of the batch exceeds the detection linlit from reduced aliquot sizes taken clue to historical process knowledge. The sample activities exceed the 11DAs. Data is accepted. Except as notedj the LCS) batch blank and sample results are within acceptance limits. Alpha Scintillation Radium-226 The achieved MDA of the samples exceeds the detection limit due insuftIcient sample volume. There is no sample volume remaining for re-analysis. Data is reported. Except as noted, the LCS, batch blank and sample results are within acceptance limits. I certify that this Certificate of Analysis is in compliance with the SO\V andlor NELAC, both technically and for completeness, for other than the conditions detailed above. The Laboratory 1fanager or a designee, as verified by the following signatnre has authorized release of the data contained in this hard copy data package. Reviewed and approved: Erika Jordan [~~~ ~~~ 2012.12.31 16:00:24 -08'00' Erika Jordan Customer Service Manager TestAmerica Laboratories, Inc. 3 Drinking Water Method Cross References -------~---------~--------I -----~---~--~-r------~~-~~~---[~~ DRINKING WATER ASTM METHOD CROSS REFERENCES ",0._._ ........... ~ .. Referenced Method Isotope(s) TestAmerica Richland'sSOP No. EPA 901.1 EPA 900.0 EPA 00-02 EPA 903.0 EPA 903.1 EPA 904.0 EPA 905.0 ASTM D5174 EPA 906.0 "'-....... -~ ....... ---... -... ---........ ------..... ... --.--.. L~.-. __ ... _ .. ~ __ ~ .. _ .. _ ...!.....--------- CS-134, 1-131 RL-GAM-001 Alpha & Beta RL-GPC-001 Gross Alpha (Coprecipitation) RL-GPC-002 Total Alpha Radium (Ra-226) RL-RA"OO2 Ra-226 RL-RA-001 Ra-228 RL-RA-001 Sr-a9/g0 RL-GPC-003 Uranium RL-KPA-003 Tritium RL-LSC-005 .~ Results in this report relate only to the sample(s} analyzed. Uncertainty Estimation TestAmerica Richland has adopted the internationally accepted approach to estimating uncertainties described in "NIST Technical Note 1297, 1994 Edition". The approach, lILaw of Propagation of Errors ", involves the identification of all variables in a11 analytical method which are used to derive a result. These variables are related to the analytical result (R) by some functional relationship, R == constants * f(x.y,z, ... ). The components (x.y,z) are evaluated to determine their contribution to the overall method uncertainty. The individual component uncertainties (Ui) ar0 then combined using a statistical model that provides the most probable overall 'Uncertainty value. All component uncertainties are categorized as type A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the components, sLlch as sample homogeneity, are combined with the component uncertainty as the square root of the sum-of-the-squares of the individual tIDcertainties. The uncertainty associated \\rith the derived result is the combined uncertainty (uc) multiplied by the coverage factor (1,2, or 3). \Vhen truee or more sample replicates are used to derive the analytical result) the type A un::;ertainty is the standard deviation of the mean value (Sl?n)) where S is the standard deviation of the derived results. The type B uncertainties are all other random or non-random components that a.re not included in the standard deviation. The derivation of the general "Law of Propagation of Errors 11 equations and specific example are -~--, -_ ... -..... --.. ....--.......... _ ................. -. --_ .. -.. . __ .... - ... _ .. _- i I ~~~ilable on reqllest:_~ ____ ~_~ __ . ___ w~ ____ ... , _____ ~ ____ ••• _____ ~ ... ----_ .... _----_._._. __ .... _. TestAmerica rptGcllcralIllfo v3.72 TestAmerica Laboratories. Inc. 4 Report Definitions r-A-c-t-:-io-n-L=--e-v-----A:-n-a-gr-e-e-:d-u-,p-o-n-a-c~ti~V17"'t-y-:-l-ev-e-:l-u-s-ed~to-tr7"ig-g-e; some action when the final resu It is greater than or equal-to the Action-- Batch Bias COCNo Count Error (#s) Total Uncert (#s) llc_ Combined Uncertainty. (#s), Coverage Factor CRDL (RL) Lc Lot-Sample No MDqMDA Primary Detector Ratio U-234iU-238 RstlM.[)C RstiTotU cel·t RcportDB No RER SDG Sum Rpt Alpha Spec Rst(s) Work Order Yield TestAmarica rptGellel-aHufo v3.72 TestAmt'!rica Laboratories, Inc. Level. Often the Action Level is related to the Decision Limit. The QC preparation batch number that relates laboratory samples to QC srunples tbat were prepared and analyzed together, Defined by the equation (ResultlExpected)-l as defined by ANSI N13.30. Chain of Custody Number assigned by the Client or TestAmerica. Poisson counting statistics of the gross sample count and backgrour.d. The uncertainty is absolute f'.nd in tr.e same units as the resuit. For Liquid Scintillation Counting (LSC) the batch blank count is the background, All known uncertainties associated with the preparation and analysis of the sample are propagated to gi ve a meaS:.lre of the uncertainty associated with the result, lie Jhe combined uncertainty. The uncertain:y is absolute and in the same units as the result. The coverage factor defines the width of the confidence interval. 1, 2 or 3 standard deviations. Contractual Requi:-ed Detection Limit as defined in the Client's Statement Of Work or TestAmerica <'default" nomina! detection limit. Often refen'ed to the reporting level (RL) Decision Level based or. instrument background 01' blank, adjusted by the Efficiency, Chemical Yiele, and Volume associated with the sample. The Type I elTOT probability is approximately 5%. Lc=( 1.645 >:< Sqrt(2*(BkgrndCntlBkgrndCntMin)/SCntMin)) l!: (ConvFctl(EffkYld*Abn*Voi) * IngrFct). For LSC rnethods the batch blank is used as a measure of the background variability. Lc cannot be calculated when the bl:'.ckgroand count is zero. The number assigned by the LIMS software to track samples received on the saJne day for a giver.. cHent. The sample number is a sequential number assigned to each sample in the Lot. Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, r,nd Volume with a Type I and II error probability ofappl'oximately 5%. MDC = (4.65 * Sqrt«BkgrndCntlBkgrndCntMin)/SCntIviin) + 2.7 liS CntMi n) * (ConvFct/(Eff '" Yid :I< Abn * Vol) :I: IngrFct). For LSC methods the balch blank is used as a measure of the background vm'iability. The lnst:'ument identifier associated with the analysis ofthe sample aliquot. The U~234 resu:t divided by the U-238 result. TIle U-2341U-238 1'£1:10 for natural Ul'fl.;'1ium in NIST SR;,Yf4321 Cis 1.038. Ratio of the Result to the MDC. A vahle greater than 1 may indicate activity above backgl'Ound at a high level of confidence. Cautio:1 s:lOuld be used when applying this factor and it should be used in concert with the qualifiers associated with tbe result. Ratio of the Result to the Total Uncertainty. If the uncerta:nty has a coverage factor of2 a value grcat{"T than 1 may indicate activ:ty above background at approximately the 95% level of confidence assuming a two-sided confidence interval. Caution should be :'lsed when <tpplying this factor and it should be used in concert with the qualifiers associated with the result. Sample Identifier used by the report system. The number is hased upon the ·first five digits of the Work Order Nurnbcr. The equation Replicate Error Ratio = (S-D)/[sqrt(TPUs2.,.. TPUd2)J as defined by lCPT BOA where S is the original san:ple resuit, D is the result of the d\lplicato, TPUs is the total uncerta:nly of the orig:nal sample ane TPUd is (he total tmccrtainty of the duplicate sample. Sample De:ivery Group Number assigned by t!ie CHent or assigned by TestAmerica upon sample receipt. The sum of the reported alpha spec results for tests derived from the same sa.11ple excluding duplicate result where the results are in tnesamc units. The LlMS software assign test specific identifier. The recovery of the tracer added to the sample such as Pu-242 used to tt'ace a Pu~239i40 method. .-... -=============================~ 5 Sample Results Sumnlnry Date: 31-0ec-12 TestAmerica Ordered by Method, Batch No., Client Sample ID. Report No. : 54130 SDG No: 46099 Client Id Tracer Batch Work Order Parameter Result +. Uncertainty ( 2s) Qua! Units Yield MOL CRDL RER2 2340044 RICHRC5011 R 1 BAG HOUSE FILTER (6067) AND MXGQT2AA TH·228 -1.75E~09 +-4.4E-08 U UCI/SA 108% B.83E-OB TH·230 /3.46E-06 +-9.6E-07 UCI/SA 10B% i.10E·07 3.00E-i5 TH-232 2.04E-08 +-4.3E-08 U UCI/SA 108% 7.74E-08 R 1 GRIZZLY FIL TER (6068) AND MXGQX1AA TH-228 1.45E-08 +-3.SE-08 U UCI/SA 115% 7.91 E-08 TH-230 v{62E-06 +-4.7E-07 UClfSA 115% 6.i6E-08 3.00E-15 TH-232 1.62E-08 +-3.4E-08 U UCIISA 115% 6.i6E-08 R 1 SYC FIL TER (6065) AND BEAK MXGQV1 AA TH-228 -2.78E-09 +-3.5E-08 U UClISA 104% 7.93E-08 TH-230 -A-.95E-06 +-5.SE-07 UCI/SA 104% 6.18E-OB 3.0DE-iS TH-232 1.63E-08 +-3.4E-08 U UCI/SA 104% 6.18E-OS R 2 SYC FILTERS (6066,6075) AN MXGQW1A TH-228 -7.36E-10 +-3.7E-08 U UCI/SA 100% 6.69E-08 TH-230 -A.56E-06 -r-4.8E-07 UCIISA 100% 6.54E-08 3.00E-i5 TH-232 O.OOE+OO +-3.6E-08 U UCI/SA 100% 6.54E-08 2340045 FFSR R 1 BAGHOUSE FILTER (6067) AND rv1XGQT1AE U-234 /3.21 E-03 +-5.7E-04 UCI/SA B1% 2A5E-OS 9.00E·i5 U-235 /1.16E-04 +-5.6E-05 UCI/SA 81% 2A5E-OS 9.OOE-i5 U-238 /3.21E-03 +-5.7E-04 UCIJSA 81% 2.4SE-05 9.OOE-1S R 1 GRIZZLY FILTER (e06S) AND iVlXGQX1AC U-234 /8.81E-05 +-4.SE-05 UCI/SA 94% 2.39E-05 9.00E-15 U-235 r4.39E-06 +-i.iE-05 U UCI/SA 94% 2.39:=-05 9.OOE-i5 U-238 .......-s.81E-05 +-4.5E-05 UCI/SA 94% 2.39E-05 9.00E-15 R 1 SYC FILTER {GOBS} AND BEAK MXGQV1 AE U-234 /5.07E-03 +-9.2E-04 UCI/SA 70% 4.18E-G5 9.0GE-iS U-235 ,)2.01 E-04 +-S.SE-05 UCI/SA 70% 3.37E-05 9.00E-i5 U-238 ,/ 5.38E-03 +-9.7E-04 UCI/SA 70% 5.39E-05 9.00E-i5 R 2 SYC FILTERS (6066,6075) AN MXGQVViA U-234 ....-2.41 E-03 +-8.3E-04 UCIISA 85% 2.33E-05 9.00E-15 U-235 .I9.25E-OS +-5.5E-OS UCI/SA 8'"01 \)/0 2.33E-05 9.00E-15 U-238 .... 2.44E-03 +-8.4E-04 UCI/SA 85% 3.09E-05 9.OOE-i5 2340042 RICHRC5011 R 1 BAGHOUSE FILTER (60(7) AND MXGQT1AD Pb-210 ../.f .12E-06 +-3.2E-07 UCI/SA 78% 3.70E-07 6.00Ep i4 TestAmerica rptSTLRchSaS'-lm mary2 VS.2.23 A2002 RER2 -Replicate ErrOl' Ratio::;; (S-D)f[sqrt(sq{TPlJs)+sq(fPOd))} as dcfincd by {CPT BOA. U Qual ~ Analyzed for but not detected nbove limiting criteria. Limit criteria Is less t:lIan the Mdc/Mda/i\'1dll Total Uliccrt, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories. Inc. 6 Report No. : 54130 Client Id Batch Work Order Parameter 2340042 RICHRC5011 R 1 SYC FILTER (6065) AND BEAK MXGQV1AD Pb-210 R 2 SYC FILTERS (6066,6075) AN MXGQW1A Pb-2i0 2340043 RL-RA-001 R 1 BAGHOUSE FILTER (60B7) AND MXGQT1 AC RA-226 R 1 SYC FILTER (6065) AND BEAK MXGQV1 AC RA-226 R 2 SYC FILTERS (60G6,6075) AN MXGQVIJ 1 A RA-226 No. of Results: 30 Smnpie Results SUlumary TestAlncrica Ordered by Method, Batch No., Client Sample 10. Result +A Uncertainty ( 2s) Qual Units ....3.46E-06 +-7.2E-07 UCI/SA .I2.78E-06 +-7.0E-07 UClfSA ...;l.20E-07 +-i.0E-07 u ./ 8.24E-08 +-1.4E-07 u Date: 31-0ec-12 SDG No: 46099 Tracer Yield MDL CRDL RER2 57% 5.33E-07 6.00E-i4 44% 7.15E-07 B.OOE-14 100% 6.62E-08 9.00E-14 51% 1.61 E-07 9.00E-14 33% 2.36E-07 9.00E-14 T estAmerica RER2 -Replicate Erl'or Ratio = (8-D}ilsqrt(sq(TPUs)+sq(fPUd»)111s defined by lefT UOA. rptSTLRchSaSum mary2 V5.2.23 A2002 U Qual -Analyzed f01' but not dctcctcdabovc limitillg criteria. Limit critedn is less than the Mdc!Mdal:\-Idl: Total Ullcert, CRDL, RDL or not identified by gamma scan software. T estAmerica Laboratories, Inc. 7 QC Results SUlumary Date: 31-Dec-12 TestAmerica Ordered by Method, Batch No, QC Type,. Report No. : 54130 SDG No.: 46099 Batch Tracer LeS Work Order Parameter Result +. Uncertainty ( 2s) Qual Units Yield Recovery Bias MDL RICHRC5011 2340044 BLANK ac, MXG752AA TH-228 -9.03E-10 +-4.5E-08 U UCIISA 98% 8.22E-OB TH-230 6.39E-08 +-7.7E-08 U UCI/SA 98% 8.81E-08 TH-232 -1.75E-09 +-4.4E-08 U UCIlSA 98% 8.81E·08 2340044.LCS, MXG752AC TH-230 2.73E-06 +-B.8E-07 J UCI/SA 121% 121% 0.2 1.28E-07 FFSR 2340045 BLANK QC, MXG771AA U-234 3.51E-08 +-1.2E-07 U UCI/SA 87% 3.30E-07 U-235 1.57E-07 +-2.0E-O? U UCI/SA 87% 3.12E-07 U-238 9.35E-OB +-1. 7E-D7 U UCI/SA 87% 3.302-07 2340045 LCS, MXG771AC U-234 6.78E-06 +-1.5E-06 UCIISA 96% 90% -0.1 2.39E-07 U-238 7.49E-06 +-1.6E-06 UCI/SA 96% 95% -0.1 2.53E-07 RICHRC5011 2340042 BLANK QC. MXG721AA Pb-21 0 7.48E-08 +-2.3E-07 U UCI/SA 76% 3.82E-07 2340042 LCS, MXG721AC Pb-21 0 9.19E-06 +-1.7E-06 UG!!SA 79% 102% 0.0 4.02E-07 RL·RA-001 2340043 BLANK QC, IVlXG731AA RA-226 4.53E-08 +-4.2E-08 U 95% 6.50E·OB 2340043 LCS, MXG731AC RA-226 1.21 E-05 +-2.7E-06 J 77% 120% 0.2 9.60E-08 No. of Results: 13 TestAmerica Bias -(ResuItlExpected)~l as dCtlllCd by ANSI N13.30. rptSTLRchQcSum .f Quul. No lJ!< qualifier has bccn assigned and the result is below the Reporting Limit, RL (CRDL) or Report VahlQ is Estimated. mary V5.2.23 U QUill -Annlyzcd for but not detected above limiting criteria. Limit criteria is less Ulan the MdcllVIda/MdJ, Total Uncert, CRDL, RDL 01' A2002 not identit1ed by gamma scall software. TeSlAmerica Laboratories. Inc. 8 -l [}!. :; ~ ;:s. ~ r ~ v o fd Q ~. :::l :> -.0 Lab Name: TestAmerica Lot-Sample No.: J2L040424-1 FORM I SAMPLE RESULTS SDG: 46099 Report No. : 54130 Client Sample ID: R 1 BAGHOUSE FILTER (6067) AND COC No.: Result Count Total MOL. Rpt Unit, Yield Rst/MDL, Parameter Qual Error ( 2 s) Uncert(:2 s} Action Lev Lc CRDL(RL} RstlTotUcert Batch: 2340042 RICHRC5011 Work Order: MXGQT1AD Report DB 10: 9MXGQT10 Pb-21 0 1.12E-06 2.5E-07 3.2E-07 3.70E-07 UCI/SA 78% (3.) i.80E-07 6.00E-14 (7.1) Batch: 234004~~ RL-RA-001 Work Order: MXGQT1AC Report DB 10: 9MXGQT10 RA-226 1.0iE-07 4.5E-08 4.9E-08 6.62E-08 100% (1.5) 3.13E-08 9.00E-14 (4.1) -----.------------ Batch: 2340044 RlCHRC50il Work Order: MXGQT2AA Report DB 10: 9MXGQT20 TH-228 -1.7SE-09 U 4.4E-08 4.4E-08 B.B3E-OB UCI/SA 108% -0.02 1.44E-08 -0-08 TH-230 3.46E-06 5.4E-07 9.6E-07 1.10E-07 UCIISA 108% (31.5) 2.62E-08 3.00E-15 (7.2) TH-232 2.04E-08 U 4.3E-08 4.3E-08 7.74E-08 UCI/SA 108% 0.26 9.89E-09 0.95 _.-.------.""~-.-.. " --.. -------.~ .. -.-.-.-- Batch: 2340045 FFSR Work Order: MXGQT1AE Report DB 10: 9MXGQT10 U-234 3.21E-03 2.8E-04 5.7E-04 2.45E-05 UCI/SA 81% (130.7) 4.01 E-06 9.00E-15 (11.2) U-235 1.16E-04 5.3E-05 5.6E-05 2,4SE-05 U'CIfSA 8'1% (4.7) 4.01E-06 H.OOE-15 (4.1) U-238 3.21E-03 2.8E-04 S.7E-04 2.45E-0!5 UCI/SA 81% (130.9) 4.01E-Oe-9.00E-15 (11.2) Ratio U-234/238 = 1.0 Date: 31-Dec-12 Collection Date: 11/27/20128:00:00 AM Received Date: 12/4/201210:15:00 AM Matrix: FILTER _____ 5?rde~~d_by Client Sample ID. Batch No. Analysis, Total Sa Aliquot Primary Prep Date Size Sizo Detector 12/28/1205:52 p 1.0 0.98619 GPC31D Sample Sample -•• --~-.~--•• ---•• ~-•• -___ "A _._ 12/30/1208:29 p 1.0 0.9862 ASC3RA Sample Sample 12/28/12 10:17 a 1.0 1.0 ALP171 Sample Sample 12/28/12 10:17 a 1.0 1.0 AlP171 Sample Sample 12/28/1210:17 a 1.0 1.0 AlP171 Sample Sample 12/20/1202:14 p 1.0 0.00109 AlP6 Sample Sample 12/20/1202:14 p 1.0 0.00109 ALP6 Sample Sample 12/20/1202:14 p 1.0 0.00109 ALP6 SHmple Sample ._. __ .•. __ ._ ... --.. --.. -•. ----... ---,.- TestAmerica MDClMOA,Lc -Detection, D~cision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample J Qual -No UI< qualifier has beon assigned and the result is below the Reporting Limit. RL (CRDL) or Report Value Is Estimated. V5.2.23 A2002 U Qual· Analyzed for but not detected above limiting criteria. Limit criteria is loss than the Mdc/Md::>/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. -i ~ ;; :3 0l n' t.l , t.l 0'" Q PJ Q rs' .~ ?> ;:; Lab Name: T estAmerica Lot .. Sample No.: J2L040424-4 FORM I SAMPLE RESULTS SDG: 46099 Client Sample 10: R 1 GRIZZLY FILTER (6068) AND Report No. : 54130 COC No.: Result Count Total MOL, Rpt Unit, Y[eld RstiMOL, Parameter Qual Error { 2 s) Uncert{ 2 s) Action Lev Lc CRDL(RLJ RstlTotUcert Batch; 2340044 RICHRC5011 Work Order: MXGQX1AA Report DB 10: 9MXGQX10 TI-I-22B 1.45E-08 U 3.5E-08 3.5E-OB 7.91 E-08 UCI/SA 115% 0.18 1.61E-08 0.83 TH-230 1.62E-06 3.3E-07 4.7E-07 6.16E-08 UCI/SA 115% (26.4) 7.B8E-09 3.00E-15 (6.9) TH-232 1.62E-08 U 3AE-08 3.4E-08 6.16E-08 UCI/SA 115% 0.26 7.88E-09 0.95 ~~-~.--.. - Batch: 2340045 FFSR Work Order: MXGQX1AC Report DB 10: 9MXGQX10 U-234 8.8iE-05 4.3E-05 4.SE-05 2.39E-05 UCI/SA 94% (3.7) 'I.B7E-06 9.OOE-i5 (3.9) U-235 4.39E-06 U 1.iE-05 1.iE-05 2.39E-05 UCIISA 94% 0.18 4.B7E-06 9.00E-15 0.83 U-238 8.81E-05 4.3E-05 4.5E-05 2.39E-05 UCI/SA 94% (3.7) 4.87E-06 9.ODE-1S (3.9) -.--~-.---.-.---~~.-.-"---~--.------, Ratio U-2341238 = 1.0 No. of Results: 6 Comments: Date: 31-Dec-12 Collection Date: 11/27/20128:00:00 AM Received Date: 12/4/201210:15:00 AM Matrix: FILTER Orderecj by Client Sample 10, Batch No. Analysis, Total Sa Aliquot Primary Prep Date Size Size Detector 12/20/12 06:117 p 1.0 O.98~39 ALP23 Sample Sample 12/20/1206:47 p 1.0 0.98439 ALP23 Sample Sample 12/20/1206:47 p 1.0 0.98439 ALP23 Sample Sample 12/20/1202:15 p 1.0 0.00119 ALP9 Sample Sample 12/20/1202:15 p 1.0 0,00119 ALP9 Sample Sample 12/20/1202:15 p 1,0 0.00119 ALP9 Sample Sample TostAmerica MDClMDA,Lc· Detection, Decision Level based on instrumont background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSamplo J Qual w No UI< qualifier has boon assigned and the result is below tho Reporting Lim(t, RL (CROL) or Report Value is Estimated. V5.2.23 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit critoria is less than the Mdclflllda/Mdl, Total Uncert, CRDL, RDL or not ldentified by gamma scan software. [i ): :::i ~ ;::;. l).) r l).) cr" o @ Q ~. :::i f> Lab Name: TestAmerica Lot-Sample No.: J2L040424-2 FORM I SAMPLE RESULTS SDG: 46099 Client Sample ID: R 1 SYC FILTER (6065) AND BEAK Report No. : 54130 COC No.: Parameter Batch: 2340042 Pb-2'tO Batch: 2340043 RA-226 Batch: 2340044 TH-228 TH-230 TH-232 ----. Batch: 2340045 LJ-234 U-235 U-238 Result Count Qual Error ( 2 s) RICHRC5011 3.46E-06 RL-RA-001 1.20E-O? U --..-_. -.-... ------- RICHRCS011 -2.78E-09 U 1.95E-06 1.63E-08 U FfSR 5.07E-03 2.01E-04 5.38E-03 4.1E-07 i.0E-07 3.5E-08 3.6E-07 3.4E-08 4.1E-04 B.2E-05 4. 3 E-04 _ •.... __ ......... --.. ,._ ... --.-~----... -""~'.--' ____ ~~v. Total MOL, Rpt Unit. Yield RstfM DL, Uncert( 2 s) Action Lev Lc CRDL(RLJ RstfTotUcert Work Order! MXGQV1AD Report DB 10: 9MXGQV10 7.2E-07 5.33E·07 UCI/SA 57% (6.5) 2.59E-07 6.00E-14 (9.6) Work Order: MXGQV1AC Report DB 10: 9MXGQV10 i.0E-07 1.61E-07 51% 0.75 7.69E-OB 9.00E-14 (2.3) Work Order; MXGQV1AA Report DB 10: 9MXGQV10 3.5E-08 7.93E-08 UCIfSA 104% -0.04 1.62E-OB ~O.16 5.5E-07 6.18E-OB UCI/SA 104% (31.6) 7.90E-09 3.00E-15 (7.) 3.4E-08 6.iBE-OS UCIISA 104% 0.26 7.90E-09 0,95 ~'-.~-.~.-----~ ... ~-~-... ----._& Work Order: MXGQV1AE Report DB [0: 9MXGQV10 9.2E-04 4.18E-05 UCIISA 70% (121.2) 9.56E-06 9.ODE-i5 tI1.) 8.BE-05 3.37E-05 UCIISA 70% (6.) 5.52E-06 9.00E-i5 (4.6) 9.7E-04 5.39E-05 UCIISA 70% (99.9) 1.56E-05 9.00E-i5 (11.1) .•. --.~------.--~" , Ratio U·234/238 = 0.9 Date: 31-Dec-12 Collection Date: 11/28/2012 8:00:00 AM Received Date: 12/4/201210:15:00 AM Matrix: FILTER Ordered by Client Sample ID, Batch No. Analysis, Prep Date 12/2B/12 05:53 p 12/30/1208:31 p Total Sa Size 1.0 Sample 1.0 Sample ---.-.--~ ---. -.... _._ ..... _-_. ----.. ----. 12/20/12 01 :42 p 1.0 Sample 12/20/12 01 :42 p 1.0 Sample 12/20/1201 :42 p 1.0 Sample 12/20/1202:14 p 1.0 Sample 12/20/1202:14 p 1.0 Sample 12120/1202:14 p 'LO Sample Aliquot Size 0.98211 Sample 0.9821 Sample 0.98211 Sample 0.98211 Sample 0.98211 Sample 0.00106 Sample 0.00106 Sample 0.00106 Sample Primary Detector GPC32A ... ---.--.~~-.. -.. - AS C6 RA ALP23 ALP23 ALP23 ALP7 ALP7 ALP? TestAmerica MDCIMDA,Lc. Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficioncy, Yield, and Volume. rptSTLRchSample J Qual M No U!< qualifier has been assigned and the result is below the Reporting Limit, RL (CRDL) or Report Value is Estimated. V5.2.23 A2002 U Qual -Analyzed fo!" but not detected above limiting criteria. Limit criteria is less than the Mdc/MdalMdl, Total Uncert, CRDLJ RDL or not identified by gamma scan software . ....... _.~_ ••• _ ,. ___ ... __ • __ ...... -" __ .0>..-__________ ._ ....... _._ •• _________ ..... __ _...-, ___ • ___ _ ~ ,/, >-~ FORM I ~. Date: 31~Dec-12 !:J ~ SAMPLE RESULTS 0-Q !:J ~ Lab Name: TestAmerica SDG: 46099 Collection Date: 11/28/20128:00:00 AM 0;' .~ Lot-Sample No.: J2L040424w3 Report No.: 54130 Received Date: 12/4/201210:15:00 AM n . Client ~ample 10: R 2 SYC FILTERS (6066,6075) AN coe No. ~ Matrix: FILTER Ordered by Client Sample ID, Batch No. Result Count Total MDL. Rpt Unit, Yield RstlMDL, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 2 $) Uncert( 2 $) Action Lev Lc CRDL(RL) RstfTotUcert Prep Date Size Size Detector Batch: 2340042 RICHRC5011 Work Order: MXGQW1AD Report DB 10: 9rvlXGQW10 Pb-?10 2.78E-06 b.1E-07 7.0E-07 7:15E-07 UCI/SA 44% (3.9) 12128/1205:53 p 1.0 0.97896 GPC32B 3.48E-07 6.00E-14 (8.) Sample Sample ------ Batch: 2340043 Rl.-RA-001 Work Order: MXGQW1AC Report DB!D~ 9MXGQW10 RA-226 S.24E-08 U 1.4E-07 i.4E-07 2.36E-07 33% 0.35 12/30/1208:25 p 1.0 0.979 ASC7HA 1.13E-07 9.00E-14 (1.2) Sample Sample 'Y--.'~-~.'--"""----'---'''-''--- Iv Batch: 2340044 RICHRC5011 Work Order: MXGQW1AA Report DB 10: 9MXGOW10 TH-228 -7.36E-10 U 3.7E-08 3.7E-08 6.69E-08 UCI/SA 100% -0.01 12/20/1206:47 p 1.0 0.97896 ALP21 8.56E-09 -0 . .04 Sample Sample TH-230 1.56E-06 3.4E-07 4.8E-07 6.54E-08 Uel/SA 100% (23.9) 12120/1206:47 p 1.0 0.97896 ALP21 8.37E-09 3.0DE-i5 (6.5) Sample Sample TH-232 O.OOE+OO U O.OE+OO 3.6E-08 6.54E-OS UCIISA 100% O. 12/20/1206:117 p 1.0 0.97896 ALP21 8.37E-09 O. Sample Sample ._--.--------~---------.. .~--.-,,--.---.-,-~.-.-~. Batch: 23400-15 FFSR Work Order: MXGQW1AE Report DB 10: 9MXGOW10 U-234 2.41E-03 2.4E-04 8.3E-04 2.33E-05 UCI/SA 85% (103.6) 12/20/1202:14 p 1.0 0.00119 ALP8 3.81E-06 9.OOE-i5 (5.8) Sample Sample U-235 9.25E-05 4.6E-05 5.5E-05 2.33E-05 UCIISA 85% (4.) 12/20/1202:14 p 1.0 0.00119 ALP8 3.81E-06 9.00E-15 (3.3) Sample Sample LJ-238 2.44E-03 2.4E-04 8.4E-04 3.09E-05 UC1/SA 85% (79.1) 12/20/1202:14 p 1.0 0.00119 ALP8 -7.621::-06 9.00E-15 (5.8) Sample Sample -----.----.----... ------.. ---.----.---. --------------.------.----.--.. --.-Ratio U-234/238 = 1.0 TostAmerica MOCIMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency. Yield, and Volume. rptSTLRchSample J Qual -'No UI< qualifier has been assigned and the result is below the Reporting Limit, RL (CROL) or Report Value is Estimated. V5.2.23 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not Identified by gamma scan software. -•..• -~~ ~ _.-, --'. ·--·· ... __ · .. ·._ ..... ·_ ..... ____ .... 1._ .... __ ._ ..... _ ... ___ •• ___ ..-_ ... _ ......... __ ..... __ .0_'. _ •• __ ._ ... __ • __ .. __ ..... ________ ...... _____ • -l :;, ~ ~ n' ~ r ~ [ p ~ (ii' ;n o I..~ Lab Name: TestAmerica Matrix: FILTER Parameter Result Qu~1 Batch: 2340042 RICHRC5011 Pb-21 0 7.4SE-OS U -p-----~.--~~~ .. - Batch: 2340043 RL-RA-001 RA-226 4.53E-08 U Batch: 2340045 FFSR U-234 3.51E-08 U U-235 1.57E-07 U U-238 9.35E-08 U -----_.-----'''-'--~'------'-' Batch: 2340044 RICHRC5011 TH-228 -9.03E-10 U TH-230 6.39E-08 U TH-232 -1.7SE-09 U --..... ---- No. of Results: 8 Comments: Count Error (2 s) 2.3E-07 4.01:-08 1.2E-07 2.0E-07 1.7E-07 4.5E-OB 7.61::-08 4.4E-08 FORM II BLANK RESUL T5 SDG: 46099 Report No.: 54130 Total MOL, Rpt Unit, Rst/MDL, Analysis, Total Sa Uncort( 2 s} Lc CROL Yield RstITotUcert Prep Date Size Work Order: MXG721AA Report DB ID: MXG721/\B 2.3E-07 3.S2E-07 UCI/SA 76% 0.2 12/28/"12 05:53 p 1.0 1.86E-07 6.00E-14 0.65 Sample -... _----Work Order: MXG731M Roport DB 10: MXG731AB 4.2E-OB 6.50E-OB 95% 0.7 12130/12 OB:28 p 1.0 3.07E-08 9.00E-14 (2.2) Sample .. ~""---'.-.~--" --...• --~.-.----.-. Work Order: MXG771AA Report DB 10: MXG771AB 1.2E-07 3.30E-07 UCI/SA 87% 0.11 12f20/12 02:15 p 1.0 8.60E-08 9.00E-iS 0.59 Sample 2.0E-07 3.12E-07 UCI/SA 87% 0.5 12/2011202:15 p 1.0 7.70E-OS 9.00E-15 (1.5) Sample 1.7E-07 3.30E-07 Uel/SA 87% 0.28 12/20/1202:15 p 1.0 8.60E-08 9.00E-15 (1.1 ) Sample Ratio U-2341238 = 0.4 ----------~-.---------- Work Order: MXG752AA Report DB 10: MXG752AB 4.5E-08 8.22E-08 UCI/SA 98% -0.01 12/2S/12 10:17 a 1.0 1.0SE-08 -0.04 Sample 7.7E-08 B.8iE-OB UCI1SA 98% 0.73 12/28/12 10:17 a 1.0 1.441::-0B 1.00E+OO (1.7) Sample 4.4E-08 B.SiE-OB UCI/SA 9B% -0.02 12/28/1210:17 a 1.0 1.44E-08 -0.08 Sample .~ •.• ·R. ___ · ___ · __ .•• ~ ~~ ..•.. _._.-.••• _ .~m __ Date: 31-Dec-12 Aliquot Primary Size Detector 1.0 GPC32C Sample 1.0 ASC9MA Sample 0.12 ALP10 Sample 0.12 ALP10 Sample 0.12 ALP10 Sample .. ----~ .. ----.--.- 1.0 ALP172 Sample 1.0 ALP172 Sample 1.0 ALP172 Sample TestAmerica rptSTLRchBlank VS.2.23 A2002 MDClMDA,Lc· Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. U Qual-Analyzed t'i>r but not detected above limiting criteria. Limit criteria is less than the Mdc!MdlllMdl, Total IJncert, CRDL, RDL or /lot identified oy gamma scan softwa.re. -~-"' ........ , ......... .-..... _-.-.--._._ ........ _. -~--••• -.. -~.-•. --------.--. --~-•. -~ -, •• &' •• _---_.-•• -.' - -•• _ ....... _. ~ .... '. ..... -' --•. ---....... --.-,. ~ ............. -_._---.... __ ........ _..-._-- -l (!) VI ? :::: ~ n' r.:.> r p) g 2 Q ~. }Il ::;l :- .J;:. Lab Name: TestAmerica Matrix: FILTER Parameter Result Batch: 2340042 RICHRC5011 Pb-210 9.191::-06 ... ---.... --.. -~,--........ Batch: 2340043 RL-RA-001 RA-226 1.21E-05 Batch: 2340045 FFSR U-234 6.78E-06 U-238 ?.49E-06 Count Qual Error (25) 4.4E-07 3.0E-07 1.1E-06 1.2E-06 ~----'-~'~-----'., ... _._ •. _---.. Batch: 2340044 RICHRC5011 TH-230 2.73E-06 5.7E-O? ------_._-----_.-No. of Results: 5 Commonts: FORM II leS RESULTS SDG: 46099 Report No.: 54130 Total Uncert{2 s) MOL Report Unit Work Order: MXG721AC 1.7E-06 4.02E-07 UCIISA Work Order: MXG731AC 2.7E-06 9.6DE-08 Work Order: MXG771AC 1.5E-06 2.39E-07 UCIISA 1.6E-06 2.53E-07 UCI/SA Work Order: MXG752AC 8.8E-07 1.28E-07 UCI/SA . _--_._--- Expected Recovery, Yield Expected Uncert Bias Report DB 10: MXG721 CS 79% 9.01 E-06 1.51 E-07 102% RecLimits: 20 115 0.0 Report DB 10: MXG731CS 77% 1.01 E-05 1.02E-07 1/.0% Ree Limits: 70 130 0.2 Report DB 10: MXG771CS 96% 7.55E-06 4.57E-08 90% Ree Limits; 70 130 -0.1 96% 7.91 E-06 4.79E-08 95% Rae Limits: 70 130 -0.1 Report DB 10: MXG752CS 121% 2.25E-06 4.56E-OB 121% Rec Limits: 70 130 0.2 Analysis, Prep Date 12/28/1205:53 p 12130/12 08:28 p 12/20/1202:15 p 12/20/1202:15 p 1?/~8/12 10:17 a .,~._~. __ ~'~M~~ ~ ••• TestAmerica rptSTLRchLcs V5.2.23 A2002 Bias -(Result/Expected)-l M defined by A.'NSI N13.30. Date: 31-Dec-12 Aliquot Size 1.0 Sample 1.0 Sample 0.13 Sample 0.13 Sample 1.0 Sample Primary Detector GPC32D ASCBMA ALP11 ALP11 ALP173 -l (t. (/; :; ::: ~ n' C) . C) ':;) ~ p) Q (5. !-". :;l r> 'oJ, ~~:~J::~.}:\~\t·~-;;:~::~::~~(;:~~~t~f~~{~~!~:?-'E~::g;;~·i:~S Chain of Custody Record TAL41?4 (1007) Temperature on Receipt __ _ TestAmerica ~blV]l'!l~l~ L2i2iB kli&£iiLiA Drinking Water? Yes 0 No 0 THE LEADER IN ENVIRONMENTAL TESTING Cliont I Proli?c! Miilfls.qer Date ChtJIn of Gustoo'v Number Tctco I Dean Kitchen. .. .11/30/2012 T~e~7:~;;~;~~~es Code)IF~Number Lab Numb9t.---.· .-..... ;~:~-.-.----'., ... '-"~f-_~-_-_!= City _ State I' Ziv Code ($'[i;-coni.;;~r·" I Lab Gantner Analysis (Attach list if Address -----. 391. East 620 South Arnencan Fork Ut ;. 84003 ; ScottChriH~n.p.n.G.rr.,nPa!m.r mora$pC:£~~4.00 __ .d'T'le_d....,O,r---'---"----; PrQi{1r;t.Mame and Location rsrai;j .. -.... -.. ~ ... -.-.. --I GanicrNVaytJi!J Number r . Denison Mine 2012 4th Quarter 1 ContractlPurcllflse Order/Quore No. Matrix .-'. -. -.--·---------1 Sample J.D. No. a.nd Descnptlon I Date 1 TIme (Containers for each sample may be combined otr OM iine)L.~~ ........ '1 ll~l~ ~ Containef.<; & Presen.rativcs ~~ • :J: ~ I- 0 N "P is :>1 rll nI g: !l Special/nstrucUof1s1 Concfitions of Receipt R 1 Bagholl," niter (GOG7) and beaker i 11/27/12 ! 8:00 tl I I I I I I I I I I I ~I~I ~1~111 I I I I ~~g; : R 1 SYC filter (6065) and beaker 11/26-28/12 8:00 :: ;~~,~:~~::::~7::: :::k::aker~:;:;;::~~.8~: '~IIIIIII 11111{1~:lxilXil ij III II +\~_--. -.-- ..... ---.. -.-." . --" ----! I I I 1-------l---I~Q~~:-:~= ~C>-.\...D\.\c)\..\~'-\ ----1 I: 1 I I I I I I I I I I ! I I I I I· t-+-·I--I --~~~, '-\ \.oh C\C\ \S~~.-. \.-\ -\2:> : l111U1II11111I1 III 1\111111111\ J2L040424 --+-----t-----t-t--I\ -I l----f---{-t----- I I I 1 I I I I 1 I I I I I I I I 1-+-1-+··-+---·--··· .. -·---·----··-------·-· r;5-..o'SPosaf By Lab Possible Hi£ard fdantification .. __ .• _____ ..1. __ . L-.... ' ~"'--" _ _'_---' _ ___'___' _ _'_--''--_'____'"--_L--''___-'-_'__ _________ _ o Non·HtlZtJrd 0 FJammab.It1 0 Skin Irritant 0 Poison B (A fee may be assessed if samples are rotoined o Archive For ___ Monlh$ (ongar than 1 month) .... ~ .•... -.-------aC,-R8q!Jirsments (Spet;if:!) o 14 Days 0 21 Days I Date 77me---.J.d~ ,,-! ....... -/ I I I _ I J a------. '-="'4. ......... -:s ,h..~'( :s:-.*L~\1--u.-\-z..1 \C)\S _ __ . __ ... ~J':: _ I lime 12.A~dBY _ . _ I Oats .1 Time' 3. ReilnquiS/led l:Iy ....... _ .. _~._._. _. __________ l~: ____ .. _ I Timl1 \3. Received By __ ~_. ___ .. __ . ______ ... __ ._-_-________ I~at8 I Tim_e __ _ Comments When Comolete Email to: Dean or Paul tetco@tetcQ-ut.c:orn i5fSTAISUTlON;' WHITE -Returned to CIi~liiViffii"fiQPor(; CANARY-Stays witn tho Sampfc;-p/f:fk Field Copy TestAmerica 15' "iI J.. mE :'5AO~R IN ENVIRONMENTAL TESllNIl Date/Time Received: \~ -~\ -\ a... \ \ ~ \S Sample Checl{-in List Container GM Screen Result: (Airlock) i>-0<6 Sample GM Screen Result (Sample Receiving) .. aD Client: ':\') Q..r.r0 Lot Number: -:Sa L.(),,-\ 0 '-\ ~ lnitial~~ ] Initials," ] SDO #:_':::\.\o-D~<'\~ __ NA [] SAF #: ______ ---..;N~ Chain ofCustody# _____________________________________ _ Shipping Container ID: ______ N~ Air Bill Nwnher: NA~ Samples received inside shipping container!coolerlbox Yes~ ] Continue with 1 through 4. Initial appropriate response. No [ ] Go to 5, add comment to #16. 1. Custody Seals on shipping container intact? Yes [ No [ No Custody Seal ~ 2. Custody Seals dated and signcd? yes [ No [ No Custody Seal ~ ] 3. Cooler temperature: ____ DC NA~ ] 4. Vermiculite/packing mateIials is NA[ \Vet [ Dry~':J ] Item 5 through 16 for samples. Initial appropriate response. 5. Chain of Custody record present? Yes~] No [ ] 6. Number of samples received (Each sample may contain multiple bottles);_~----,, __ 7. ~~~~~~~~~M~-~~_U_\~~~t~;~\~~~~~---------____ _ 8. Sample holding times exceeded? 9. Samples have: __ tape 10. 11. __ custody seals Matrix.: . __ A (FLT, Wipe, Solid, Soil) ~S (Air, Niosh 7400)' ,. f ~ \1...-\,.\-\"'1- ~mples: are in good condition __ are broken NA[ Yes [ hazard labels ~ appropriate ~~m~l~ labels ~I(Water) ~_T (Biological, Ni-63) __ are leaking ___ have air bubbles (Only for samples requiring no head space) ____ Oth& __________________________________________________________________________ __ ~". 12. Sample pH appropriate for analysis requested Yes = ] No [ ] NA ~~ ] (If acidification is necessary, then doct:.ment sampl::! ID, initial pH. amount ofH:-.IOJ added ~Jd pH after addition on table overlea;j RPL ID # of preservative used : ______ _ 13. \Vere any anomalies identified in sample receipt? Yes [ 1 No ~ ] Description of anomalies (include sample numbers): NA ~ ________ _ 14. LS-023, Rev. 15,07/11 See over for addiiional informatiOll. T ~stAmerica Laboratories, Inc. 16 TestAmerica ~ Vm:UIIWl'il!llllilf THE !.E"OER IN ENVIROt!'oIf.N,. ... L TES-m'IG 15. Sample Location) Sample Collector Listed 011 coe? ... *f-or documentation only. No corrective action needed. Yes~] No[ 16. Additional Information: _________ . _______________________ _ [ ] ClientiCourier denied temperature check. Sample Custodian: t. C). > ~ ~ Client/Courier unpack cooler. Date: \ 'cl. -\...\ - \ "'L Client Infonned on. ________ ':ly _________ Person contacted _________ _ p(J No action necessary; process as is Project M.nager£~~ Q~ate r2. .. -4--1-'"2- I SA.i\1PLE ID Initial pH Acid Amt Final pH ~LEID Initial pH Acid A.T'llt Final pH \ I ~\ I \. -\, \ \, I \ \, '\ I \ .. \\ \ \,. I I .. '\ I V/.) ! \. " ,~------\ ---<'-x\tf \, /'] 1 K( ,j(t. \ '~/ ! \ I \, "\' \ \ I '\. _.-.--.-~ I \ I \\ \\( \ \/\1 '\k I \~\I \ ". \f \ '~.) .\ 1 I '\ I i I \ i \ I I ! i ! i , ! i \ \, i ~ I \ i : \\ ! \ I I I ! I I l I -_ .• '------- LS-023, Rev. 15,07/11 See over for additional information. Tl;!stAmerica Laboratories. Inc. 17 APPENDIXD South Yellow Cake Scrubber Figure 1. Facility Schematic Representation Yellow Cake Dryer Baghouse Figure 2. Facility Schen1atic Representation Grizzly Baghouse Figure 3. Facility Schetnatic Representation Production and Control Equipment Data South Yellow Cake (Scrubber Flow Rates) Yellow Cake Dryer Baghouse (Delta P readings on Field Data Sheets) Grizzly (tph ofn1aterial and beltspeed) o Facility: Energy Fuels Resources t ex, ! y Stack Identincation: SOllth Yellow CaJ<e Scrubber 1~0~1 , . p a: Distance upstream from next disturbance, feet ~: Distance downstream from last disturbance, feet y: Distance of Sample Level to Ground, feet 0: Stack Inside Diameter, inches Estimated Moisture, percent Estimated Temperature, of . Estimated Velocity, fpm Control Unit Type: Scrubb(.'r Number of Ports ~ T -------------------- 30' 65' ------------------ 12.75" ------------------- 4-8 '100-120 -------------------- 3.000 ------------------ ") .::., I.:'igure I. Facility Schematic Representation Process Type: Yel !(nv Cake Processing Facility: Energy Fuels Resources t ex ! y Stack Identification: Yellow Cal(eDryer .Bag.l1.0tISe 1+-0~1 II a !3 ex: Distance upstream fi·om next disturbance, inches 57" -------------------- 13: Distance downstream from last disturbance, inches 45411 y: Distance of Sample Level to Ground, feet 65' ------------------ 0: Stack Inside Diameter, inches 16" -------------------- Estimated Moisture, percent 0-2tyo Estimated Temperature, OF 125 ------------------- Estimated Velocity, fpm 1 A·OO Contl'ol Unit Type: 13aghoLlse Number of Ports 2 oIf Figure 2. Facility Schematic Representation Process Type: Yellow Cake Processing Facility: Energy Fuels Resources t . a ! y Stack Identification: Grizzly BagJl0l1se 1~0~1 . , f3 a: Distance upstream from next disturbance, inches 24.5" --------------------- 13: Distance downstream ii"om last disturbance. inches .:18" 2R' y: Distance of Sample Level to Ground, feet ------------------ 0: Stack Inside Diameter, inches ! 8.7511 ------------------- Estimated Moisture, percent 1%) Estimated Temperature, of Ambi~nt ------------------- 775 Estimated Velocity, rpm ______________ _ Number of Ports 2 Process Type: Control Unit Type: ...---'--------..... Ore Unloading and C()f1v(~ying ~ Bughouse Figure 3. Facilitv Schematic RCDresentation Energy Fuels Resources, Blanding, UT Process Data Source: South Yellow Cake Date: / /-,2. 6-' /:z.. Scrubber Flow GPM Time #1 #2 l\P I (l: 'i (-;; )v. Cj It? 7 ! iF:(t? )#. c:7 ! p. 7 ;J..t(?J J~ 1 ! Cj'~ 7 /tf:/C ;J),}. /0. 7 11.'it? }/'7 /~'7 17;(0 ,,3 )./ 4 /iJ, 7 17 ~ &( () ) l. -7 IC· 7 /1-;7-fj-) " /)-)J(~ /p< 7 1 I ,,! ,,/ \V \J 7 : y)r-) 2..; (; I tJ. 7 Q '( ,.--:J J, ) It/, 7 (;9 • ) j/: tfy-) /1 7 /~ 7 1.'(;-J-cr, ~ Iv, 7 -1 ru ,-. (J -.' I-P' (/- --'7 i. lJ-,-) ., I / '-~ " i.-,~ .,) /'7. !.... -1 1.-1 ,.. ))' .. 0 1~.7 !.-,."/ l . t-} . './ 32-,7-/o'T />.) . .::;. ... / "" "'" .. , ( I- f) , L f / ~/ (.... .. ' : , f -.. ~-(,) ,7.J~ ( 10-7 " ::;, ) ~! .---) )( 0 I CJ' 7 c/ I ,.,. ' --, . -. .,.-) ) , ~ Energy Fuels Resources, Blanding, UT Process Data Source: South Yellow Cake Date: ,. /-/ ["//1 I t r il' ~ Scrubber Flow GPM Time #1 #2 6P J(},')Q ? ]r:L Iv.? ) / ,t () () ;;;;.. £. / t:P, 7 , //c') 0 :;).~ /0\7 I}.·' (/0 ;;~ ( /V',7 !)l")() .J)/b /~I '7 /) .4 (Jt/ 3)r ~ IcP.7 /) ,e ) (; )~,\ lO·1- J vi: OU ~-;;') IO·:L / (.t~· ) 0 ~1-D \ J '1- lJ~'OcJ J'L, z.,.. 16·+ 1./~'30 71. L ( 0·1- le.( C/o ~"5. ~ ( 0 ~i /&/){) ) ,. u 10' T /7 ~( CO Energy Fuels Resources, Blanding, UT Process Data Source: Grizzly 8aghouse I' • \ . Time ()o I l . ~~ .. t....-. > u Tons (Integrator) J L l .2. :0 Date: tph I l 0 .. / i I ') l ~ . /' lC ) fpm I c, G. cy • '-..l 'J \. /0 8· 8 l r-·., (J "'/0' I U ; I I APPENDIXE Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and ten1perature sensors \vere calTied out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 4 Schematic of Method 5/114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-test Dry Gas Meter Calibration Data Forms Type S Pitot Tube Inspection Data San1ple Box Ten1perature Sensor Calibration E Temperature Sensor t ~probe Type S Pitot Tube Tempe~ature Temperature Sensor Nozzle H:.>atT~ sensor~ Gooseneck ! ~ GJa;s.finro / Prcbe --~ Glass FHter / ~ ~.--91 Holder Type S Pitot ~ I I Heated Area Tube Stack Wall Manometer Implnger Train Optional, May 8e Replaced 8)' An Equivalent Condenser I Temperature Sensor ,-- ---- -------- lmpingers Air-Tight Pump Figure 4 Schenlatic of Method 5/114 Sanlpling Train METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of lime necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the :,~Ht::EU cells. YELLOW cells are calculated. METER SERIAL #:!--'--'-'=-"-'-_ CRITICAL ORIFICE SET SERIAL #:1 1453S EQUIPMENT 10 #: K' TESTED ...-----...----11 FACTOR !VACUUM G G G RUN # I (AVG) 0.8137 0.8137 0.8137 0.5317 2 0.5317 0.5317 0.3307 0.3307 0.3307 lin Hg) 13 13 13 13 13 13 13 13 13 548.140 553.420 558.698 564.820 570.025 575.265 581.802 • 587.303 : 592.812 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 553.420 558.698 564.244 570.025 575.265 580.513 587.303 592.812 598.325 5.280 5.278 5.546 5.205 5.240 5.248 5.501 5.509 5.513 75 73 15 73 75 75 75 76 75 80 75 81 75 84 75 86 15 81 73 73 75 76 76 80 80 82 81 84 83 85 86 88 87 86 89 81 76 80 83 84 85 87 86 87 89 Facility FINAL 25.30 ELAPSED ::l TIME (MIN) AVG 0 73.75 5.00 16 5.00 18.50 5.25 80.50 1.50 82.50 7.50 84.00 1.50 8G.00 86.50 88.00 ~1r ~~~ ENVIRONMENTAL SUPPLY COMPANY AVG(Pb .. ) 25.3 2.90 2.90 2.90 1.20 1.20 1.20 § 0.44 0.44 New Calibration 2012 4.4546 ~ llill. ~ ~ ~ ~ ~ ~ IF V VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALl BRA TED 1 4.4515 0.999 ~ .1..&Qi !:ill!! 1:.!!Q!! AVG= ~ ~ ~ 1.,Q11 ~ 1:.!!Q!! ~ ~ AVG = .J..,QQ2 .Qda ~ .:J..,QQ1 ~ 1J!Ql ~ 1.006 AVG= .:J..,QQ1 ~ 1.136 .l.,ll2 .1:.ill 1:§.§1 .1&1l ~ .1M! lSI 1.542 The following equations are used to calculate the standard volumes of air passed through the DGM. V", (sid). and the critical orifice, VI.! (std). and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 1.006 (1) (2) (3) 1"111""" =K. * VIII * I'h(/r+(/!J.flII36) Tm J'(.'J"{ ~"/, ,,' .. /'h',I,.* (-) J'iillllh = Net volume of gas sample passed through DGM, corrected to standard conditions 1<, = 17.64 aRlin. Hg (English). 0.3858 GI<Jmm Hg (Melric) T" = Absolule DGM avg. temperature (oR· English, OK -Metric) '" Volume of gas sample passed through the critical orifice. corrected to standard conditions T'n,b = Absolute ambienl temperature ("R • English. oK· Metric) K' = Average K' factor from Critical Or.iflce Catibration ""';""1 r=---= DGM calibration factor "/11",.1, Pre Calibration 2008 AVERAGE AHm =/ 1.641 ~HC!!= ( 0.750 )2 AH (Vm(std)\ Vc.(std) v... ) Temperature Sensors Reference In Out OF OF OF 34 67 202 35 68 203 35 68 203 ...... METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES _d/f4QiiM@mw... _j!!~ ::! 1) Select three critical orifices to calibrate Ihe dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feel. 4) Record data and information in the GREEN cells, YEllOW cells are calculated. METER SERIAL #:1-"'::':"':";;";;'--1 CRITICAL ORIFICE SET SERIAL #:1 14535 EQUIPMENT 10 #: 1(' TESTED r----------~ FACTOR I VACUUM G G G RUN# I (AVGI 0.8137 0.8137 0.8137 0.5317 0.5317 0.5317 0.3307 0.3307 0.3307 (inHg) 13 13 13 13 13 13 13 13 13 110.501 118.685 118.G8S 125.253 125.253 131.839 74.902 80.511 80.511 86.136 ~~.13_S_. _ --.!.1.ns __ 92.1010 97.376 97.376 104.211 104.211 109.766 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 8.184 6.568 6.586 5.609 5.625 5.639 5.275 G.835 5.555 72 72 72 72 72 72 72 72 ,-_?2 87 88 89 75 80 83 85 85 86 87 87 88 88 89 89 77 75 80 80 83 83 65 85 85 85 86 87 __ 87 88 89 78 80 83 85 85 ~- INITIAL FINAL AVG (Ph.,) 25.5 25.5 ELAPSED TIME (MIN) 0 r-- 87 7.50 2.60 88 6.00 2.50 89.00 6.00 2.60 76.25 8.00 ~ 80.00 8.00 1.12 83.00 ~ 85.00 12.00 85.00 15.50 8S.50 12.50 r;.:;2 ~ 5.4348 5.4397 4,7229 ~ ~ 4.3615 5.6514 4.5804 2012 Pre-Calibration IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 1 6.7490 !bill 5.3992 0.993 ~ ~ AVG= 0.994 -0.50 ill1Q. 0.996 4.7040 1.000 ill1Q. ~ AVG= .1.:Q.Q.Q. !!.Jl 4.3886 ~ 5.6686 1.003 4.5715 0.998 AVG= 1,QQl !!d!! The following equations are used to calculate the standard volumes of air passed through the DGM, V m (sid), and the critical orifice. Vcr (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 0.999 (1) (2) (3) 1'111""" = 1\1 * r'lI/ >I< Phew .j-( All / 13.6) 7ill Phar *l:> Vcr",.!, == K '", -"J7~;;/~i; = Net volume of gas sample passed through DGM, corrected to standard conditions K, = 17.64 DR/in. Hg (English), 0.3858 DKlmm Hg (Metric) Tin = Absolute DGM avg, temperature (OR -English, OK -Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T .n •. = Absolute ambient temperature (OR -English, OK -Melric) 1(' = Average K' factor from Critical Orifice Calibration I'Cli,'d, r ..... -.-.. = DGM calibration factor /'//1",,1, AVERAGE ~H(!!! =1 1.493 2 ~H(!!! = (0.750) ~H (Vm(std») Vc,(std) Von Temperature Sensors Reference In Out ~ ~ OF 33 67 201 34 67 202 34 67 202 M!! 1.494 :!.&Z 1.534 1.524 1.515 !MQ. 1.460 Lill. PRE Console #4 Calibration 2012 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select Ihree critical orifices 10 calibrate the dry gas meier which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run al tested vacuum (from Orifice Calibration Report), for a period of time necessary 10 achieve a minimum total volume of 5 cubic feel. 4) Record data and information in the cells, YELLOW cells are calculaled. K' I TESTED .-----..----11 FACTOR VACUUM [:] G G RUN# I IAVG) 0.8137 2 0.8137 0.8137 0.5317 2 0.5317 0.5317 0.3307 0.3301 ~-?307 (inHg) 12 12 12 13 13 13 20 20 20 METER SERIAL #:1-1 --=":":;';;~-l CRITICAL ORIFICE SET SERIAL #: 857.685 863.696 863.696 869.730 869.730 875.755 840.0900 845.380 845.380 850.723 850.723 856.048 800.747 806.875 806.875 812.608 812.608 817.910 G.011 6.034 6.025 5.290 5.343 5.325 S.128 5.733 5.302 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: H H H 75 75 75 G8 68 68 ~ ~ ~ ~ ~ 100 ~ ~ 1M 82 85 91 85 87 92 87 89 95 75 79 75 79 80 81 80 83 84 100 1M 1~ 92 95 98 81 84 83 1, ~J:::, .. ~; --:f.'!' 2012 Pre-Calibration INITIAL FINAL AVG (Pb .. ) 25.45 25.45 IF Y VARIATION EXCEEDS 2.00%. ORIFICE SHOULD BE RECALIBRATED ELAPSED I ! ::l AVG !T1ME:MINI 94.25 5.50 2.55 4.9075 !.lli1 !:.QM 1.460 96.25 5.50 2.55 4.9085 4.9257 1.003 !:.ill 98.25 5.50 2.55 4.8836 ~ 1.009 1.450 AVG= 1&Q§, 0.12 87.50 7.50 1.11 1..lli1 i:ill!!. 1.008 1&Q1 89.75 7.50 1.11 4.3797 4.3890 1.002 1.494 92.25 7.50 1.11 4.3451 4.3890 ~ 1.488 AVG= 1&QI Q.4Z 77.50 14.00 0.40 5.1272 5.1293 i.COQ. 1.402 81.00 13.00 0.40 4.7656 i:Iill ~ 1.393 82.50 12.00 0.40 ~ 4.3966 MQQ. 1:1M AVG= 1.000 ::!h1Q The following equations arc lIsed to calculate the standard volumes of air passed through the DGM, V m (std), and Ihe crilical orifice, Vcr (sid), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheel above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 1.004 (1) (2) (3) '·II/I'/.l':= 1\1 *1"1/1* Pbal' + (L\{1113.6) Till Vcr, ,J.! I Ph",. * (;;) K'~-"h~';lIh = Net volume of gas sample passed through DGM. corrected 10 standard conditions KI = 17,64 °R/in. Hg (English). 0.3858 °Klmm Hg (MetriC) T", " Absolute DGM avg, temperature (OR -English, oK" Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T ... ,., '" Absolute arnbienttempemtufc (OR -English, °1< " Metric) K' = Average K' factor from Crilical Orifice Calibration "CI; w-}' =~ "._-,.------. ;: DGM calibration factor 1'111,,,.,, AVERAGE t\H@=1 1.448 t\H@= 2 ( 0.750) L\H (Vm(std») Vcr(std) VIn Temperature Sensors Reference In Out OF OF OF 32 33 32 72 73 73 203 202 202 Pre 2012 5 console METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the <;;F:ELN cells. YELLOW cells are calculated. METER SERIAL #:1 ._-----I CRITICAL ORIFICE SET SERIAL #: L..' ___ --' EQUIPMENT 10 #: K' TESTED FACTOR I VACUUM I RUN # I (AVG) (in Hg) DGM AVG Facility FINAL 25.45 ELAPSED TIME (MIN) o <IIIIIIIIIII~!!: . . ~.- .'1-~~ l: ENVIRONMENTAL SUPPLY COMPANY Energy Fuels Resources AVG (Pb .. ) 25.45 North Yellowcake Dryer Baghouse IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 1 D:rn~ .0 III , , ... , .0 .0 o o 0.00 §§ 0: 0.6808 13 0.6808 13 0.6808 13 755.104 760.818 760.818 766.566 766.566 __ 272.361 _ D:rn~ USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 5.714 5.748 5.795 .0 .0 .0 70 62 67 67 74 70 67 70 74 77 70 70 74 77 80 1-~,nlml'l 67.50 72.00 75.25 0.00 0.00 0.00 6.50 1.95 6.50 1.95 6.50 1.95 §§ AVG= 4.8933 4.8934 1.000 4.8807 4.8934 1.003 4.8907 4.8934 1.001 AVG= 1.001 AVG= The following equations are used to calculate the standard volumes of air passed through the OGM, V m (std), and the critical orifice. Vcr (std). and the DGM calibration factor, y, These equations are automalicallycalclliated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = r-1.()o-i--1 (1) (2) (3) 1'111",,,,;::;; K, * Vm*tbar+(IlH 1\3.6) 7in I',.,. A.' '", j)/l(//' >I< 0) , ,," '-1/~~~:F/'- = Net volume of gas sample passed through DGM, corrected to standard conditions Kl ::; 17.64 °R/in. Hg (English), 0.3858 °Klmm Hg (Metric) T m ::; Absolute DGM avg. temperature (OR -English, oK -Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T.mb::: Absolute ambient temperature (OR -English. OK -Metric) K':: Average K' factor from Critical Orifice Calibration /'CI;"d, r "" -;--- 1-111,,,,/. = DGM calibration factor Pre Calibration 2008 AVERAGE AH@ =C1~645--1 2 AH@ = (0.750) AH (Vm(std») Vc,(std) VOl Temperature Sensors Reference In Out OF 34 67 202 OF 35 68 203 OF 35 68 203 0.00 1.657 1.643 1.633 U;J METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES ~i1t11tilM'itMWlj&lilirt@. # Ut'11~lj -!;!J ;i'-e--+ 1) Select three critical orifices to calibrate the dry gas meier which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. Facility Energy Fuels Resources Grizzly 4) Record data and information in the GREEN cells, YELLOW cells are calculated. FINAL AVG (Pb.,) 25.45 25.45 METER SERIAL #:c:=J CRITICAL ORIFICE SET SERIAL #:~ EQUIPMENT 10 #: K' TESTED FACTOR 1 VACUUM RUN# (AVGI (in Hg) G: 0.5317 13 0.5317 13 0.5317 13 237.605 242.814 242.814 248.050 _2'!13-050 253.294 ---- D:B~ D:B~ USING THE CRITICAL ORIFICES AS CAUBRA TION STANDARDS: 5.209 5.236 5.244 .0 .0 .0 .0 .0 .0 ELAPSED TIME (MIN) a 70 69 71 70 75 71.25 7.50 1.10 70 71 74 75 77 74.25 7.50 1.10 70 74 74 77 77 75.5 7.50 1.10 '--. I Il-fll:: §§ '--'-l--'· ~··l-' :::: § § 4.418 4.416 Mll IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 1 4.41 0.998 4.41 0.998 4.41 0.999 AVG= 0.999 0.00 AVG= AVG= The following equations are used to calculate the standard volumes of air passed through the DGM, V m (std), and the critical orifice, Vcr (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 0.9991 (1) (2) (3) VII/I,M) ::: 1\, * VIII * _~!Ulr + (AN 113.6) 7~;;----'--' Phar * (':') 1\'*-_.-=-Ver\.".!, == ~JJtb = Net volume of gas sample passed through DGM. corrected to standard conditions K, = 17.64 °R/in. Hg (English). 0.3858 °Klmm Hg (Metric) T m = Absolute DGM avg. temperature (OR -English, oK -Metric) = Volume of gas sample passed through the critical orifice, corrected to standard conditions T.mb = Absolute ambient temperature (OR -English, oK -Metric) " K' = Average K' factor from Critical Orifice Calibration Vel;"./) y=--= DGM calibration factor 1'111(".1) AVERAGE AH@ =[1~1-1J 2 AH(fl) = (0.75 0) AH (V m(std)) Vcr(std) Vm 1.518 .1&1Q .1:.QQ2 Post test #4 Calibration 201? t~JJ _.:... METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1I111lll1!--III!I1l-Ifi~~~~~~iiji!!l!H!!~!!1 I~;'-'·-:.\ il!11i17lJiillW; MW1lW1PittfY07fi'._ ,j".\l!: ii. r--~)1n,!, " 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated. Facility Energy Fuels Resources South Yellowcake Dryer Scrubber FINAL AVG (Pb.,) METER SERIAL #:}--";;";"';";"':";;--i CRITICAL ORIFICE SET SERIAL #:1 14535 EQUIPMENT 10 #: 25.35 25.35 IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED K' TESTED FACTOR I VACUUM RUN# I {AVG} (in Hg) 0.6808 13 0.6808 13 0.6808 13 56.523 62.732 62.732 69.992 69.992 75.30 0: 0.5317 13 0.5317 13 0.5317 13 75.30 80.550 80.550 85.845 85.845 91.151 G: D:~~ USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 6.209 7.260 5.308 5.250 5.295 5.306 .0 ,0 .0 ro N ~ ~ n ro ~ ro n ~ , ro _ 7~ n ~ u 70 75 77 75 79 70 77 79 79 84 70 79 80 84 87 ,--I-I'·· fJ 67.5 72.25 76.25 76.50 79.75 82.50 0.00 0.00 0.00 ELAPSED TIME (MIN) e 7.00 1.90 7,00 1.90 7.00 1.90 7,50 1.10 7.50 1.10 7.50 1.10 §§ 5.2956 5.2491 0.991 6.1367 5.2491 0.855 4.4533 ~ 1.179 AVG= 1.008 4.3924 4.3923 1.000 4.4033 4.3923 0.997 4.3901 4.3923 1.001 AVG= 0.999 AVG= The following equations are used 10 calculate Ihe standard volumes of air passed Ihrough the DGM, V m (SId). and the critical orifice. V rJ (sId). and the DGM calibration factor, Y. These equations are automatically calculaled in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = 11.0~04-1 (1) (2) (3) VIII(.-I") = Kl * VII/ * Pbar -I-(1\11113.6) 7in - Pbar * e Vcrl .• ,.!, ::;;: K'* -JTamb = Net volume of gas sample passed through DGM, corrected to standard conditions KI = 17.64 OR/in. Hg (English). 0.3858 °Klmm Hg (Metric) To, = Absolute DGM avg. temperature (oR· English. OK -Metric) = Volume of gas sample passed through the critical orifice. corrected to standard conditions Tamb = Absolute ambient temperature (oR· English, OK -Metric) K' = Average K' factor from Critical Orifice Calibration 1"0; ,'.}l }' =, .... --= DGM calibration factor 1'lIlr,ld) AVERAGEhH@=11.5541 2 hH@= (0.750) hH (Vm(std) Vc,(std) Vm 1 0.45 -0.45 1.621 1&QI ~ 1.51 1.50 1.49 posl test 20125 console Dat;!. (2,.. -\1.. -1 \ flO, h U ..... ~---J.., a~ , Type S Pi tot Tube Inspection Data Pltot Tube! fd~ntification __ ~--...:_ ... _( _Jr::=-______ _ OF • p ... = . 4 ~l> in. ~------~--------- p,! = .'i'O Ctl" !O" a!" 100 In. Is P", = Po? "I-e.-.3> ------~----------Is 1.05· Dt ::; D: ::; 1.50· D\ '? _\..-'-(_e---__ ~ ____ _ ~! = ---"---- Z~O.125in. Z= .QV( in. w ~ 0.03125 in \V::: 00 t.1 in \V> 3 inches w-:=. <ok m z > 3/4 inch Z== 11 ~ m. -.•..... " ..q:= y ~ 3 mchcs ~--~~~I ~--!---------. y = _3"",,---h_'Zbo<-__ m The f.ltul tube meets the spr:cifi~atlons for a c:tlIbrJtion factor oro 8·.1" "I.e..~ TCmpCfdtlJrC Sensor Calibration T c!Olpcraturc TCnJocrature I Temperature Sour.;:e Rderencc Sensor II DlfTcrllnce (~kdlUrn) ! C'F) (F) II (oF) AIR (p( f.p"'/ ~ Pr,)bc ConUnUlty 'P H~Jt Ched: ~~8 ;r--7 V-c.....~ I l,§(O AIR If (PS" cpt{ . I ICE V':t\TER f, ')"t. 3' i ... t ! Slack 'BOll \VATER '\,.0 "'V 4..-0 \ I \ ! SILICONE OIL I --~-.. ---i C: r--j ~ A ) \" /' (~\ I S I L. _ ___' .... '.--...~ c::: Anl --3 ( .. -.--=--~ ~ \.._-------~ ~, C2 Z -~I-'­ I r.--------:::or--.....---.."\'\ L _________ ~ ,c:::~~~;.::.·~i.:-\\ 1 I ~ .~~-"IIIi' .. f-----i'~:c;:,~~ [~~-, ... -.J.-... : nu 1 \' c ... __ ~F_. __ "_·<_"_'·'_'·'~ Pltot Tube: J..:knlif'(Jtion ___ 2...:.:::.......:.1 ________ ' Dr-II 1.' S in r.t!' I')') (!:= ___ L ___ _ (!~ , ! :y' (!: :.:: ___ '1---.;:.. __ _ ZSOl25in f)! .: __ "'--=-_ P:=--\-- \\' S. 0 03125 In W= -030 ir. \\' ';.. 3 inch~s W= ~ \lz.. in z > 3/·~ Ir:ch z"" "!t( Is p.l.:: p 8 ': _Y-,,-C-__ S __ _ \(~S ----- f~~~~~~,:~U [ j_ .. ; .. ,. += _' _____ y:: :; i::d1~S y :::: __ L_' ____ H1 Cl I T ~----~- '--'-;---/' ~ p). W-i--.-~,; __ ____l~_PB Afol --_./:\ j ~~; ---~ ~--~ ~.--.. -.-.-. -"'~ '-..J.... ()2 .,----z ---JI"""'-l: L-.. ~-~ \\. -.. ..:.. .. -.. -~ .. -.. -.!"-.. -. T;. pc S Pitot Tube Inspc...:{ion Oatl Pl ... ~t TUD:! lJ;!:1t;!k:!:iNl ""2... l -~ T;;-chnician K. ,....I\..{. MO\.....V\A.~ P •. '"' • y 1...1 Sin. p~= U 43> 1:: (L, < I'l (!: = __ --'-__ _ <..:: <: I;)~ 0.; "'-__ --=0::...-__ z ~ 0.125 ill W S 0.0:;125 in W> 3 inches \\'= .:1 ;(1 Z-= \ in S~J~~ rt()rr. \\' .. \ TER 5!LCCC):\"EOIL j , r---- II ... -J I z ~-'-r­ ( » ~ ... ~.J ..... ___ _ r="'~c~~~-_-~ : I.V)" f :. '····t'1,~1 ~~i' J l I:, .,." .•.. ,~ 0 Type S Pitol Tub~ Insp~cti:)n D:lt:l PJ,,~t Tube I,~e:lt:::·::!::(\n ~ S I -" &r Te.:h:tt.:i:l:1· \(. M GMt>.. Vv\.~ .. • ""2.-~D in '1t;(P in. p~ =. ·3S(P I~ (!: -:; 1':,0 (:;::: C!.; < 10" Ct.: =---4---- PI < 5~ 0: =. 0 0; < 5' !l: = 0 z $ 0125 in 7.= W::;003125 in \,. - \V >.3 inch~:i \\'= t; iI., ----.:"----- z'" I \/"L-in (~~~~~J-' ... ,':' -<1-__ y ~ :; ir:ch.:s y= ___ L[+-__ ir. F:0b~ S~_"'.~~ T :::})~~;J.:~';:;! S~:--d,)r CJ!;br~~:ct~ R·~:"'':i~::~''': I AIR I~\ I k~ I ICE W,,\TL:R ~ \ 1"1 'I \",.,..,.." ! 2nS I "LoS I ::»!~ ••• ..... H.:C'. 15E .. ICO\::. on, I II t 1 . II ! 1 ! Ii TETCO Sample Box Temperature Sensor Calibration Date: 12/29111 Calibrator: Kawai McNamara --------------------------------Reference: Omega CL3511A Unit ID Temperature Temperature Temp Diff Thermocouple or Re' su·lt· Source Reference I Sensor Location () (oF), PfF" (Medium) ("F) ( F) Oven It-_w_ate_r --I111----33-/It--33---lII----oo-------=l . Water .. 205 .. 205 . A Probe Out II'"' ---~-·-:-~:-~---~II-I------;-~)-----In 1----2- 3 0- 3 5-----11'" -----~---~ Oven B Probe Out ,1~----~-J:-:-~---~III---------;-~)------~I~I-----2-~-~------4I~-------O-l------q Impinger Out Oven 2 o c 2 Probe Out o Impinger Out -I Oven D Oven E Probe Out Irl------~-,:-:-~------il~-------;-~-5------~I~------2-~-~-----~II-----~-;----~ Oven F Probe Out Irl---w-w-:-::-~---il'"------}-~2-----ill--·------2-~-~------;1I-------_-~----~ APPENDIXF The testing followed the san1e procedures as outlined in previous protocols and tests at this facility_ ATTACHMENT H SURF ACE WATER GRAPHS AND FIELD DATA SHEETS 1.00E-05 1.00E-06 1.00E-07 a;-n; ~.OOE-08 en o ::::!. 1.00E-09 1.00E-10 1.00E-11 • OjCO~ ~~ ~ • ~ ~t-..Oj q}rf Cottonwood Creek Dissolved Radionuclide Concentrations (uCi/ml) • OjOj~ ~~ t-..rV'" • ~ ~O:J \l-~ R>CO ~t-..Oj q}ro ~ t-..~ • U-Nat. -Th-230 • Ra-226 • R> ~\:5 t-..~ ~ t-..~ ~~ t-..~ 1.00E-06 1.00E-07 1.00E-08 :i' m ~.OOE-09 C) o ..J - 1.00E-10 1.00E-11 1.00E-12 R><O ~~Oj ~~ ...... • .. -----, " Cottonwood Creek Suspended Radionuclide Concentrations (uCi/ml) • ..... " -" ----" -- 2>~ ~~Oj ~~ I -~ • " .... -... • ..... ... .. • .... • .... ~ . ...... ..... " .. -• 2><0 ~~Oj ~~<r;j ~rv • • • • • •• • ... -- ~ .... .... .... ... ... .-•• ••••••• •••••• " ~~ ~~~ ~co ~ ~ ~~ • U-Nat. -Th-230 ~ Ra-226 I - ---- ... -i ~ ••• ~ " --- ~~~ ~~ ~t\;. t(\ ~~ ~~ EI'fRGY L ABORATORIES www.energylab.com Analytical ExcsthmcB SinCll 7952 Helena, MT 877 .. 412 .. 0711 • Billings, MT 800 .. 735 .. 4489 • Gasper, WV 888 .. 235 .. 0515 -~iilette, WY 866-686-7115 • Rapid City, SI} 888-672-1225 • College station, TX 888-690-2218 ANALYTICAL SUMMARY REPORT September 25, 2012 Energy Fuels Resources (USA) Inc 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C12081141 Project Name: 3rd Quarter Surface Water 2012 Energy Laboratories, Inc. Casper WY received the following 3 samples for Energy Fuels Resources (USA) Inc on 8/28/2012 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix C 12081141-00 1 Cottonwood Creek 08/24/12 9:30 08/28/12 Aqueous C 12081141-002 Cottonwood 65 08/24/129:30 08/28/12 Aqueous C12081141-003 Temp Blank 08/24/12 0:00 08/28/12 Aqueous Test Sample Filtering Uranium, Dissolved Uranium, Suspended Digestion, Total Metals Gross Alpha minus Rn222 and Uranium Radium 226, Dissolved Radium 226, Suspended Thorium, Isotopic Thorium, Suspended Isotopic Solids, Total Dissolved Solids, Total Suspended Same As Above Temperature The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: c5¥~D uJ~~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.09.25 10:37:17 -06:00 Page 1 of 13 www.~nergylab.com Analytical ExcsllsncB Sines 1952 Helena, MT 877·472-0711 • Billings, MT 800-735·4489 . Casper, WY 888-235-0515 Gillette 'NY 866-686·7175 • Ra id Ci ,SO 888-612·1225 . Colle e Station IX 888-690-2218 CLIENT: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Surface Water 2012 Report Date: 09/25/12 Sample Delivery Group: C12081141 CASE NARRATIVE RA226 ANALYSIS USNRC Regulatory Guide 4.14 provides guidance on Minimum Detectable Concentrations (MDC) that should be achieved in samples for this radionuclide. The sample-specific MDC for this sample could not be achieved due to significant matrix interferences, restricting the volume of sample to be used in the analysis. Please consult with your local regulatory agency prior to using these results for compliance purposes. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-cs -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 13 EI\ERGY LABORAT ORIES www.energylab.com Analytical ExceUsncs Sincs J 952 Helena, MT 877 -412-0111 • Billings, MT 800-735-4489 • Gasper, WY 888-235-0515 Gillette, WY 8&&-&86-7175 • Rapid City, SO 888-&12-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Surface Water 2012 Lab ID: C12081141-001 Client Sample ID: Cottonwood Creek Analyses PHYSICAL PROPERTIES Solids, Total Dissolved TOS @ 180 C Solids, Total Suspended TSS @ 105 C METALS -DISSOLVED Uranium METALS-SUSPENDED Uranium RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC RADIONUCLIDES -SUSPENDED Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 329 1260 0.0017 0.0035 3.1 1.8 2.1 0.53 0.28 0.33 7.2 1.2 0.2 4.4 0.49 0.28 3.1 0.9 0.6 Units mg/L mg/L mg/L mg/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pC ilL pCilL pCi/L pC ilL MOC -Minimum detectable concentration Report Date: 09/25/12 Collection Date: 08/24/1209:30 DateReceived: 08/28/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date / By 0 10 A2540 C 08/29/12 15:30 1 jz 60 A25400 08/29/12 14:59 1 jz 0.0003 E200.8 09/14/12 11 :45 1 cp 0.0003 E200.8 09/18/12 22:401 cp E900.1 09/07/12 07:261 Ibb E900.1 09/07/12 07:261 Ibb E900.1 09/07/12 07:261 Ibb E903.0 09112/12 15 :55 1 dmf E903.0 09112/12 15 :55 1 dmf E903.0 09112/12 15:551 dmf E908.0 09/11/12 08:59 1 dmf E908.0 09/11/12 08 :59 1 dmf E908.0 09/11/12 08:591 dmf E903.0 09118/12 01 :28 1 dmf E903.0 09118/12 01 :28 1 dmf E903.0 09118/12 01 :28 1 dmf E908.0 09/17/12 10:261 dmf E908.0 09117/12 10:261 dmf E908.0 09117/12 10:261 dmf MCL -Maximum contaminant level. NO -Not detected at the reporting limit. o -RL increased due to sample matrix. Page 3 of 13 EI'ERGY LABORATORIES www.energylab.com Analytical ExcsllBfICB Sincs 1952 Helena, MT 877-412-011 1 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~illette, Wy 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Surface Water 2012 LablD: C12081141-002 Client Sample ID: Cottonwood 65 Analyses PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C Solids, Total Suspended TSS @ 105 C METALS -DISSOLVED Uranium METALS -SUSPENDED Uranium RADIONUCLIDES -DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC -See Case Narrative regarding Ra226 analysis. RADIONUCLIDES -SUSPENDED Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 391 1400 0.0019 0.0030 0.8 1.4 2.1 0.01 0.28 0.51 0.3 0.2 0.2 4.0 0.53 0.35 1.7 0.6 0.5 Units mg/l mg/L mg/L mg/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/l pCi/l pCi/l pCi/l pCi/l pCi/L pCi/L pCi/L MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration Report Date: 09/25/12 Collection Date: 08/24/12 09:30 DateReceived: 08/28/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By D U U 10 A2540 C 08/30/12 16:101 jz 60 A2540 D 08/29/12 14:59 1 jz 0.0003 E200.8 09/14/12 11 :49 1 cp 0.0003 E200.8 09/18/12 22:451 cp E900.1 09/07/1207:26/1bb E900.1 09/07/1207:26/1bb E900.1 09/07/1207:26/1bb E903.0 09112/12 17:27 1 dmf E903.0 09112/12 17:27 1 dmf E903.0 09112112 17:27 1 dmf E908.0 09/11/12 08 :59 1 dmf E908.0 09/11/12 08:59 1 dmf E908.0 09/1 1/1208:591 dmf E903.0 09118/12 01 :28 1 dmf E903.0 09118/12 01 :28 1 dmf E903.0 09118/12 01 :28 1 dmf E908.0 09117/12 10:261 dmf E908.0 09117/12 10:261 dmf E908.0 09117/12 10:261 dmf MCL -Maximum contaminant level. ND -Not detected at the reporting limit. D -RL increased due to sample matrix. Page 4 of 13 EN:RGY LABORATORIES www.enerl!lllabocom (' Analytical ;;csnsnel Sines 1952 J. Helena, MT 877-472-0111 • Billings, MT 800-735-4489 '" Casper, WY 888-235-0515 ~ille.tt¢, WY866-686-7175 fII Rapid City, SD 888-672-1225 .. College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Surface Water 2012 LablD: C12081141-003 Client Sample ID: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: RL -Analyte reporting limit. QCl -Quality control limit. Result Units 506 Qualifier RL Report Date: 09/25/12 Collection Date: 08/24/12 DateReceived: 08/28/12 Matrix: Aqueous MCL! QCL Method Analysis Date / By E17001 08/28/12 09:20/ kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 5 of 13 EN:RGY LABORATORIES www.energy]ab.com Analytical Excellence Sines 1952 Helena, MT 871 .. 412-0111 • Billings, MT 800 .. 735-4489 • Casper, WV 888-235-051 5 . ',~ille~e, WY 8&& .. &86-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Surface Water 2012 Analyte Count Result Units Method: A2540 C Sample 10: MB-1_120829A Method Blank Solids, Total Dissolved TDS @ 180 C ND mg/L Sample 10: LCS-2_120829A Laboratory Control Sample Solids, Total Dissolved TDS @ 180 C 1070 mg/L Sample 10: C12081138-002AMS Sample Matrix Spike Solids, Total Dissolved TDS @ 180 C 2180 mg/L Sample 10: C12081168-001 A OUP Sample Duplicate Solids, Total Dissolved TDS @ 180 C 1310 mg/L Method: A2540 C SampledO: MB-1_120830A Method Blank Solids, Total Dissolved TDS @ 180 C ND mg/L Sample 10: LCS-2_120830A Laboratory Control Sample Solids, Total Dissolved TDS @ 180 C 1090 mg/L Sample 10: C12081135-001A MS Sample Matrix Spike Solids, Total Dissolved TDS @ 180 C 1150 mg/L Sample 10: C12081191-005A OUP Sample Duplicate Solids, Total Dissolved TDS @ 180 C 30000 mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration RL 10 10 10 10 10 10 10 10 Report Date: 09/25/12 Work Order: C12081141 %REC Low Limit High Limit RPO RPOLimit Qual Batch: TDS120829A Run: BAL-1_120829A 08/29/12 15:20 Run: BAL-1_120829A 08/29/12 15:20 96 90 110 Run: BAL-1 120829A 08/29/12 15:30 99 90 110 Run: BAL-1 120829A 08/29/12 15:32 - 0.6 5 Batch: TDS120830A Run: BAL-1_120830A 08/30/12 16:06 Run: BAL-1_120830A 08/30/12 16:06 98 90 110 Run: BAL-1 120830A 08/30/12 16:09 - 91 90 110 Run: BAL-1 120830A 08/30/12 16:12 - 2.8 5 ND -Not detected at the reporting limit. Page 6 of 13 EN:RGY LASORAT ORIES www.energylab.com Analytical Excel/snee Since 1952 Helena, MT 877 -472-0711 .. Billings, MT 800-135-4489 -Gasper, 'NY 888-235-0515 GiII~tte, WY866 .. 686-7175 • Rapid City, SO 888-672-1225 .. College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Surface Water 2012 Analyte Count Result Units Method: A2540 0 Sample 10: MBLK1_ Solids, Total Suspended TSS @ 105 C Method Blank NO mg/L Sample 10: LCS1_ Laboratory Control Sample Solids, Total Suspended TSS @ 105 C 191 mg/L Sample 10: C12081137-003AOUP Sample Duplicate Solids, Total Suspended TSS @ 105 C NO mg/L Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Report Date: 09/25/12 Work Order: C12081141 RL %REC Low Limit High Limit Run: BAL-1_120829B 60 Run: BAL-1_120829B 6.0 95 60 110 Run: BAL-1 120829B 6.0 NO -Not detected at the reporting limit. RPO RPOLimit Qual Batch: R163991 08/29/12 14:57 08/29/12 14:57 08/29/12 14:58 5 Page 7 of 13 EI\ERGY www.energylab.com Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 _GiII~tte, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, 1)( 888-690-2218 LABORATORIES Analytical Exesllance Sines 7952 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Surface Water 2012 Report Date: 09/25/12 Work Order: C 12081141 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E200.8 Sample 10: ICV Uranium Method: E200.8 Sample 10: MB-34899 Uranium Sample 10: LCS2-34899 Uranium Sample 10: C12081141-0020MS Uranium Sample 10: C12081141-0020MSO Uranium Method: E200.8 Sample 10: ICV Uranium Method: E200.8 Sample 10: LRB Uranium Sample 10: LFB Uranium Sample 10: C12081091-001AMS Uranium Sample 10: C12081091-001AMSO Uranium Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Initial Calibration Verification Standard 0.0504 mg/L 0.00030 101 Method Blank NO mg/L 0.00030 Laboratory Control Sample 0.0996 mg/L 0.00030 100 Sample Matrix Spike 0.106 mg/L 0.00030 106 Sample Matrix Spike Duplicate 0.112 mg/L 0.00030 112 Initial Calibration Verification Standard 0.0504 mg/L 0.00030 101 Method Blank 0.00114 mg/L 0.00030 Laboratory Fortified Blank 0.0515 mg/L 0.00030 101 Sample Matrix Spike 0.0517 mg/L 0.00030 100 Sample Matrix Spike Duplicate 0.0523 mg/L 0.00030 101 Analytical Run: ICPMS2-C_120918A 09/18/12 13:25 90 110 Run: ICPMS2-C_120918A Run: ICPMS2-C_120918A 85 115 Run: ICPMS2-C_1 20918A 70 130 Run: ICPMS2-C_120918A 70 130 5.5 Batch: 34899 09/18/12 22:32 09/18/12 22:34 09/18/12 22:48 09/18/12 23:02 20 Analytical Run: ICPMS4-C_120913A 09/13/12 14:20 90 110 Batch: R 164629 Run: ICPMS4-C_120913A 09/13/1215:12 Run: ICPMS4-C_120913A 09/13/12 15:17 85 115 Run: ICPMS4-C_120913A 09/14/12 10:52 70 130 Run: ICPMS4-C_120913A 09/14/12 10:57 70 130 1.1 20 NO -Not detected at the reporting limit. Page 8 of 13 EN:RGY LABORAT ORIES www.energylab.com Analytical Exestlsncil Sines '852 Helena, MTB77-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, lX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Surface Water 2012 Analyte Count Result Units Method: E900.1 Sample 10: LCS-GA-0581 Gross Alpha minus Rn & U Laboratory Control Sample 23.2 pCi/L Sample 10: MB-GA-0581 Gross Alpha minus Rn & U 3 Method Blank Gross Alpha minus Rn & U Precision (±) Gross Alpha minus Rn & U MDC Sample 10: C12081275-002GMS Gross Alpha minus Rn & U -0.539 pCi/L 0.435 1.03 pCi/L pCi/L Sample Matrix Spike 55.3 pCi/L Report Date: 09/25/12 Work Order: C12081141 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: BERTHOLD 770-1_120906A 117 80 120 Run: BERTHOLD 770-1_120906A Run: BERTHOLD 770-1_120906A 132 70 130 Batch: GA-0581 09/07/1207:26 09/07/1207:26 U 09/07/1207:26 S -Spike response is outside of the acceptance range for this analysis. Since the LCS and the RPD for the MS MSD pair are acceptable, the response is considered to be matrix related. The batch is approved. Sample 10: C12081275-002GMSO Gross Alpha minus Rn & U Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Sample Matrix Spike Duplicate 55.4 pCi/L U -Not detected at minimum detectable concentration Run: BERTHOLD 770-1_120906A 09/07/1207:26 30.5 128 70 130 0.1 NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 9 of 13 EN:RGY LABORATORIES www.energylab.com (1:' . Analytical Exest/snell Sines 1152 L ~'. , L .. ~., Helena, MT877-472-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 .~illette, WY 866 .. 686-7175 • Rapid City, SO 888-672-1225 .. College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Surface Water 2012 Analyte Method: E903.0 Sample 10: LCS-RA226-6211 Radium 226 Sample 10: C12081277-001FMS Radium 226 Sample 10: C12081277-001FMSO Radium 226 Sample 10: MB-RA226-6211 Radium 226 Radium 226 precision (±) Radium 226 MDC Method: E903.0 Sample 10: LCS-34864 Radium 226 Sample 10: MB-34864 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: C12081141-00100UP Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: C12081141-0020MS Radium 226 Qualifiers: RL -Analyte reporting limit. Count Result Units Laboratory Control Sample 6.5 pCi/L Sample Matrix Spike 14 pCi/L Sample Matrix Spike Duplicate 14 pCilL 3 Method Blank -0.11 pCi/L 0.078 pCi/L 0.19 pCi/L Laboratory Control Sample 12 pCi/L 3 Method Blank 0.098 pCi/L 0.12 pCi/L 0.19 pCi/L 3 Sample Duplicate 4.4 pCi/L 0.52 pCi/L 0.32 pCi/L Sample Matrix Spike 57 pCi/L MDC -Minimum detectable concentration Report Date: 09/25/12 Work Order: C12081141 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: BERTHOLD 770-2_120905A 105 80 120 Run: BERTHOLD 770-2_120905A 107 70 130 Run: BERTHOLD 770-2_120905A 105 70 130 1.7 Run: BERTHOLD 770-2_120905A Run:G5000VV_120910B 102 85 115 Run:G5000VV_120910B Run:G5000VV_120910B 0.0 Run:G5000VV_120910B 113 70 130 NO -Not detected at the reporting limit. Batch: RA226-6211 09/12/12 15:55 09/12112 15:55 09/12/12 15:55 25.6 09/12/12 19:00 U Batch: RA226-6222 09/18/12 01 :28 09/18/12 01 :28 U 09118/12 01 :28 33.1 09118/12 01 :28 U -Not detected at minimum detectable concentration Page 10 of 13 EN::RGY LABORATORIES www.energylab.com Analytical ExCIJIIsnCB Sines 1952 Helena, MT 877·472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 .~ille&e, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, DC 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: 3rd Quarter Surface Water 2012 Analyte Count Result Units Method: E908.0 Sample 10: LCS-RA-TH-ISO-1693 Thorium 230 Laboratory Control Sample 3.3 pCi/L Report Date: 09/25/12 Work Order: C12081141 RL %REC Low Limit High Limit RPO RPOLimit Qual Run:ALPHANALYST_120907A 63 80 120 Batch: RA-TH-ISO-1693 09/11/1208:59 S -LCS response is outside of the acceptance range for this analysis. Since the MS, MS, MSD, and all tracer recoveries are acceptable the batch is approved. Sample 10: C12081268-002CMS Thorium 230 Sample 10: C12081268-002CMSO Thorium 230 Sample 10: MB-RA-TH-ISO-1693 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Method: E908.0 Sample 10: LCS-34826 Thorium 230 Sample 10: MB-34826 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Sample 10: C12081141-0020MS Thorium 230 Sample 10: C12081141-0020MSO Thorium 230 Qualifiers: RL -Analyte reporting limit. 3 3 MDC -Minimum detectable concentration Sample Matrix Spike 11 pCi/L Sample Matrix Spike Duplicate 11 pCi/L Method Blank 0.033 pCi/L 0.075 pCi/L 0.18 pCi/L Laboratory Control Sample 11.1 pCi/L Method Blank 0.1 pC ilL 0.1 pCi/L 0.3 pCi/L Sample Matrix Spike 47 pCi/L Sample Matrix Spike Duplicate 45 pCi/L U -Not detected at minimum detectable concentration Run: ALPHANALYST_120907A 94 70 130 Run: ALPHANALYST_120907A 97 70 130 2.9 Run:ALPHANALYST_120907A Run:ALPHANALYST_120911C 107 80 120 Run: ALPHANAL YST _120911 C Run: ALPHANAL YST _120911 C 118 70 130 Run: ALPHANAL YST _120911 C 114 70 130 3.8 NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. 09/11/1208:59 09/11/12 08:59 40.4 09/11/1209:00 U Batch: R164775 09/17/12 10:25 09/17/1210:26 U 09/17/12 10:26 09/17/12 10:26 45 Page 11 of 13 EN:RGY LABORAT ORIES ~. '1~" WVi'W.energylab.com .:, ~ Analytical Exes/IBnCil Sines '152 Helena, MfS77 -472-0711 · Billings, MT 800-735-4489 11 Casper, WY 888-235-0515 Gillette, WY 866-686-7175 11 Rapid City, SD 888-612-1225 11 College Station, IX 888-690-2218 Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Energy Fuels Resources (USA) Inc Login completed by: Timothy I.. Houghteling Reviewed by: BL2000\kschroeder Reviewed Date: 9/6/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottie? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Temp Blank received? ContaineriTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: Yes 0 Yes D Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 5.6"C On Ice Yes D Yes 0 C12081141 Date Received: 8/28/2012 Received by: th No D No D No D No D No D No D No D No D No D No D No D No D No D Carrier NDA name: Not Present D Not Present 0 Not Present 0 Not Applicable D No VOA vials submitted 0 Not Applicable D Samples were split, filtered, and preserved as necessary for dissolved and suspended parameters. Page 12 of 13 "U Q) co CD --\. W o ---\. W EN:RGV mJ mao Chain of Custody and Analytical Request Record Page -L of --L- • -......... -........... , .............. -.-.......• "~ ••••••• "'., ................... ~,.,.. ... v.N'.v·L Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: EI\~r-.0Y Fvt.,..\S .3t"~ D vo-..r-i'u-.svr~~{,Gr tJe... .. er ~ State: tli Yes 1St No 0 10- Report Mail Address: P ... O. (0)C ~Oq Contact Name: Phone/Fax: Email: Sampler: (Please Print) 13"~~~ 1 ()T'" 'I.fSII (;-A.r,.; A. P600.tM-U'" ~3S 11' "'~;tl G#J~'fI'tw P~.J~~ Invoice Address: Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: S~yV\..e. S A"v\. ~ Special ReportJFormats: ~ ~ W@U@ OO~®QD§@lJ~lID • Contact ELI prior to ~"U/s:.gD4 0 .... RUSH sample submittal ~O(l)~ ~ for charges and Cooler 10(5): ~ee~OI~ ~ ~ C R scheduling -See Ctl~J-._> 0 >-m '-w t:.. Instruction Page o OW 0 EOD/EDT(Electronic Data) ~(I)~ m 3: ~ .~ :J: o~= Yd CD ~ "C Receipt Temp o POTVVf\NWTP Format: U c: Comments: ~~~I.Q~ 1 :::J U o .... eel c:: ~ ~ ~ e ~(p °c o State: D LEVEL IV •• CD 'C::: ~ as f'c.A.S~ (:1\ tV' ~ (1)-50 ~ c (9N o Other: 0 NELAC .8~I~ ~ ~ S fr-c..Sc.r-\Je.. On Ice: Er-So...e • io ::J :::J Q)--CD 3: l-S zc..~lafC V1 ...q \oil ~ ~ W "2 AS t'\ c.c..cl. ~ • Custody Seal fij >1 V ~ ,,~ ~ W {g On Bottle D= (I) e tv ~ -,: (J) C On Cooler -.. ~ ~ to J.. f (j) H Intact Y N SAMPLE IDENTIFICATION Collection Collection ~ ~ MATRIX ~ ~ ~ Signature Y N (Name, Location, Interval, etc.) Date Time ~ Match 1 X ~ X X .~ G.."t-""OA..ltVo.lk L.r-~ gI1",,1I2.. "4:30 1-"J '.>( ~ 2l:,C++OAWOOo\ 6~ i12JiLt:l. _Q9'30 lor W X X X )( X )( I~ 3 ~ Innn 4 ]I 5 '0;::::1 ~ 6 bo~J''''(( 7 ~ 8 ~. 9 ~ 10 1r::JJ Oatemme: DatafTime: Custody Relinquished by (print): Signature: Received by (print): Signa re: If".~r-;A. P~'~&t"" IJ1..f,j},4...J HdO ~-PM,.--Record Relinquished by (print): MUST be Signed Sample Disposal: DateITIme: Signature: Reoeived by (print): DatefTime: Signature: l<I:ecelV8G uy LaooralOry: ~atefllme: L \:>Ign~ Return to Client: Lab Disposal: ;;t. V -) -:l... 2~ 2-;;; I pies suomtuec to t:nergy Laooratones, Inc. may be subcontractea to otner cenrneCl laooratorles In oroer to complete me analy This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. -_.--.• _-.1_'----1:--_ ..... 1: .. : ___ 1 :_$ .............. ; ............. ,., ... I","" ... !lIihlo foa ctl"hal'lllloPo fnrm~ Ann IinkR. LLL. .L IT,/, ."" I' White Mesa Mill -Standard Operating Procedures Book #11: Environmental Protection Manual. Section 2.1 Date: 2/07 Revision: DUSA-I Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle oneXS§tonwood C~ Westwater Canyon Other (describe) ____ _ DATE: g/l L.II J 2 pH BUFFER 7.o __ 7.L..:..>-...:::o:::;.... ... ') __ _ BY: brr;/>-PAL"",eC &. P. (Sampler's initials) pH BUFFER 4.0 __ Y-,-"-,, 0"'-· ... ·_) __ SPECIFIC CONDUCTIVITY _q....l-.....Lq-Jq'--_____ I.l=M.:.=.::H~O=s STEAM DEPTH: _ ........ 1 £.0,£5--'-\ _____ _ pH of WATER _7.j-<e=-.tf..w:-( ...... : _______ _ COND !lmhos 2D 1 ,r 0 pH Units --7{-.:.-q..l...g~. __ _ Temp °C _ ....... /.....;.7-'-.--'C, ....... f_· __ COND !lmhos 2D J • D pH units i. 0 D Temp °c J r~ 0 '1 Comments: TEMPI5bL~ • I CONDllmhos ;;L06 .. 3 pH units S',-o I COND Ilmhos 20 I .. f pH units f~ D ::( Temp °c 11. 20 or;,.ry rj':cl-y .. -re-!Mfc.£e..-h/,..c:. !/tt,$ 1£"4 A..J.. .10&"",/ ~t-'i-Le +-~M.t.. a{:' 'L-e..~+-s~·te.. ~+ C?<1i.-!~.., CiJl.r1pi; ~ .. , White Mesa Mill -Standard Operating Procedures Book # 11: Environmental Protection Manual, Section 2.1 Date: 2/07 Revision: DUSA-l PageS ofS Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION {Circle one):Cottonwood Creek QVestwater Can;Qll)Other (describe) ____ _ DATE: 5f /:2Li / 11. pH BUFFER 7.0 _---.j7 ....... "'u..Oo::;..,-__ _ BY: bo...rr;o.A.: Pc..lyV':e,r: 6: . .p (Sampler' s initials) pH BUFFER 4.0 --+Lf'"'-'w.o~-- SPECIFIC CONDUCTIVITY _q.L-1.L-'1J--_____ ~u=MH=O::...:::.s STEAM DEPTH: --.......tY"'--':A'-'--______ _ pH of WATER __ N<..;....L.A ________ _ TEMP __ ~lS~O~L~ ____ _ < 1 COND J::::! .. lI=nhO;::::.:S::_._ ___ _ COND "Il=mh==.:;os"--___ _ pH Units ________ _ pH units _______ --- Temp °c ______ _ Temp °c _______ _ COND~rr.ili==;::::.:os::_._ _____ __ COND Il,=mh=os::_._ ___ _ pH units ______ _ pH units _______ _ Temp °c __ ~ __ Temp °c ______ _ Comments: r.t/-:Ly/i'b ALr'lqul ¢>A. ,ae... ?\..}. lOOP" tr~e...t L.?c""S cAci, fl', bzre..! wee" h"k.-tAt 9 /, 7' /1 A rr'i II e.~. 60......fl + e. ,,??OQr L \,e,e. JL W c.... s J..t-'Ii ,0;-L -t () Te ( W tee +v--.Ke V\~ 9/27/; 2 Arrluu>.. t;?A-{'(t·t I~+-ot3Q e t-re.e..-JL w~_~ cAr'ye " .. White Mesa Mill-Standard Operating Procedures Book # 11: Environmental Protection Manual, Section 2.1 Date: 2/07 Revision: DUSA-l Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one)€ttonwoo~ Westwater Canyon Other (describe) ____ _ DATE: 12./711:Z BY: U:4.U;oA.. &..1~.e..c / tiP (Sampler's initials) I pH BUFFER 7.0 __ 7~. 0 ____ _ pH BUFFER 4.0 __ r;J-L~~O~ __ SPECIFIC CONDUCTIVITY __ q,,--, q.&-q-'---____ -"Jl=M=H~O=s STEAM DEPTH: ALA pHofVVATER _____________________ _ TEMP _______ _ , ) COl\lJ) =umh=o-=-=s"--___ _ COND~rr.ili==o~s~ ____ __ pH Units ______ _ pH units ______ _ Temp °C ______ _ Temp °C ______ _ COND~mh==o~s~ ____ __ COND~=rr.ili=o=s~ _____ _ pH units ______ __ pH units ______ _ Temp °c ______ _ Temp °c ______ _ Comments: p~tD" Arr")Cd?\. db $:+<: M OBI5 ""'" .tL/Pi/la, f..r".e:e.\c. WAr tArt Ar ... ,vc.q\ C""-(,TL a... ...... 08""5 i1'/'-o ,a.la.,ht .. Lr-e.s.k.. wa,S bey Se.e c...tt~kL.-c..rA (~oh:;,j. , White Mesa Mill-Standard Operating Procedures Book #11: Environmental Protection Manual, Section 2.1 Date: 2/07 Revision: DUSA-I Page 5 of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one):Cottonwood Creek ~twater Can]2iDOther (describe) ___ _ DATE: 1.2/7/12.. BY: 6:-4rej.A.. (?t;",tvY'-ec !?:l? (Sampler's initials) ( pH BUFFER 7.0 _......;7t...J!,,~O~ __ _ pH BUFFER 4.0 _--..:Y-=...;' 0""'--__ SPECIFIC CONDUCTIVITY _q-#.-.-l-,--Lq _____ ---'=u~M=H~O=s STEAM DEPTH: pH ofWATER __________ _ TEMP ____________ __ • I COND=Mmh==~OS~ ______ __ COND~=mili=o~s~ ______ __ pH Units ______ _ pH units ________ _ Temp °c ______ _ Temp °c _______ _ COND~rr.ili==~os~ ____ __ COND~=mili~os~ ____ __ pH units _______ _ pH units _______ _ Temp °C __________ _ Temp DC ______ _ Comments: Ar,.;".,..r!. (>& ,:-ilk ed· Q9$D. frt;.cr;".., :.1 4.....A.V ,I"( (CAi c...Cc.c ~ sJ&( ,)..r=y, Je.1!.. p~h> Art-,ve-A ,/It. .s;te.. "'-t 09"0 b.A la/,t.f/'.g\ L.ret~ k,)"",S Dry-Arl"'vd t:lA-£: f c... ~t 0 130 <> A. I p.,J {J. ,I j P. t..re-e. k IA.l4J Art r Arl' ~ v e.e:\ tVA. S. .'J<!. ~ + ~/~ OA.. .:z./ (L6t ,P.. .. c... r-c..e..lc-Vt.)A-..s D,..y. (po".,.-t?--+-.J.e~p-J.s f,;Ve.re: lODG> M-p..,J,.t:-Pvf &r~erlc.--bl.:Lc.e..use. pk""~ ~~ l~/7 ol~p{-,\+ -h.-rV\. tflvf tAJ~t..:; ATTACHMENT I SOIL SAMPLE GRAPHS, DATA TABLE, LABORATORY RESULTS AND QAlQC + III I f + III I -;::: I\.) + III I -;::: w + III I -;::: ~ + III I < cJ, + III I -;::: 0> Jul-98 Oct-98 Jan-99 Apr-99 Jul-99 Oct-99 Jan-OO Apr-OO Jul-OO Oct-DO Jan-01 Apr-01 Jul-01 Oct-01 Jan-02 Apr-02 Jul-02 Oct-02 Jan-03 Apr-03 Jul-03 Oct-03 Jan-04 Apr-04 Jul-04 Oct-04 Jan-OS Apr-OS Jul-OS Oct-OS Jan-06 Apr-06 Jul-06 Oct-06 Jan-O? Apr-O? Jul-O? Oct-OJ Jan-08 Apr-08 Jul-08 Oct-08 Jan-09 Apr-09 Jul-09 Oct-09 Jan-10 Apr-10 Jul-10 Oct-10 Jan-11 Apr-11 Jul-11 Oct-11 Jan-12 Apr-12 o o (]'I ......10. (]'I Jul-12 I ••••• I • N N (]'I w w (]'I :::tJ su c. c: 3 I I\) I\) 0) o o ::l (") (I) ::l r+ Sil r+ o· ::l tn ::l en 2. -"C o ::::::.: (Q - t CO I f + co I c;::: N + co I c;::: w t co I c;::: ~ + co I c;::: (J'J + CO I c;::: CJ) o o 0'1 0, I'V I'V 0'1 w JUI-98 I .1. I . .. I. Oct-98 Jan-99 Apr-99 Jul-99 Oct-99 Jan-OO Apr-OO Jul-OO Oct-DO Jan-01 Apr-01 Jul-01 Oct-01 Jan-02 Apr-02 Jul-02 Oct-02 Jan-03 Apr-03 Jul-03 Oct-03 Jan-04 Apr-04 Jul-04 Oct-04 Jan-05 Apr-05 Jul-05 Oct-05 Jan-06 Apr-06 Jul-06 Oct-06 Jan-07 Apr-07 Jul-07 Oct-07 Jan-08 Apr-08 Jul-08 Oct-08 Jan-09 Apr-09 Jul-09 Oct-09 Jan-10 Apr-10 Jul-10 Oct-10 Jan-11 Apr-11 JUI-11 Oct-11 Jan-12 Apr-12 Jul-12 I •• '. .' • :e W 0'1 ~ ~ 0'1 c D1 :::J C 3 I Z Q) r-o o :::J o CD :::J r+ D1 tr. o :::J tJJ :::J en 2. -"tl o :::: (C - 9/7/80 9/8/81 12/3/81 6/30/82 5/5/83 6/4/84 10/12/8 4 8/28/85 8/1/86 8/17/87 8/28/88 8/25/88 8/1/90 8/5/91 8/13/92 8/13/93 8/3/94 8/28/95 8/13/96 8/1/97 7/1198 8/24/99 12/1/00 8/23/01 0.650 0.400 0.790 0.423 0.471 0.713 2.960 1.630 0.369 0.600 1.500 1.200 2.900 3.900 1.200 2.000 1.000 2.810 1.700 0.540 1.600 2.270 1.510 1.000 0.420 1.800 0.770 0.384 0.410 0.866 0.886 0.800 0.654 0.800 1.600 1.600 5.800 8.800 2.200 1.700 1.600 4.700 2.150 0.310 3.050 1.740 1.210 1.000 0.340 0.300 0.440 0.412 0.569 0.618 2.330 2.190 0.466 1.500 1.300 1.100 1.000 1.700 0.900 1.400 0.700 0.680 0.600 0.560 0.700 0.780 0.810 0.600 WHITE MESA MILL Soil Sampling Results (VALUES) x 10-3 uCi/kg 0.420 0.600 0.560 0.l80 0.550 0.683 0.069 0.424 0.866 0.900 0.700 3.000 1.400 2.600 1.400 1.700 0.800 0.200 0.460 0.l60 0.580 0.840 0.530 0.300 0.420 0.300 0.890 0.265 0.461 0.489 2.880 2.270 0.382 0.800 0.600 0.800 0.800 2.600 0.800 1.100 0.700 0.880 0.300 0.410 0.500 0.530 * 0.400 0.420 0.600 0.420 0.207 0.340 0.471 0.721 0.424 0.694 0.600 0.900 1.000 1.400 5.700 1.200 1.900 0.900 0.650 0.210 0.270 0.450 0.420 * 0.300 0.410 0.200 0.750 0.478 0.643 0.l24 3.490 4.330 0.396 1.200 1.000 1.100 1.800 1.800 0.900 0.800 0.700 0.580 0.500 0.410 1.000 0.840 0.830 0.900 12.194 3.000 0.630 0.260 0.340 0.324 0.804 0.294 0.826 0.700 1.300 1.400 1.300 2.600 0.900 1.600 1.100 0.240 0.520 0.260 1.190 0.770 1.220 1.000 0.230 0.300 0.550 0.449 0.l47 0.l32 2.550 1.280 0.728 1.500 3.800 2.900 3.700 2.500 1.100 4.800 3.000 2.800 1.900 1.700 3.000 3.270 2.810 1.200 14.89 1 0.600 0.420 0.216 0.l40 0.310 0.817 0.577 0.836 1.300 5.000 5.700 3.200 4.400 1.800 3.500 3.800 1.600 2.010 1.500 2.760 3.150 3.250 1.100 8/1/02 1.300 1.350 0.900 0.524 0.500 0.297 1.200 1.490 2.400 2.810 60.00 0.550 8/5/03 0.800 0.990 0.600 0.790 0.500 0.330 0.600 0.4300 0.280 0.420 0.600 0.530 8/9/04 0.600 0.610 0.400 0.250 0.400 0.220 0.600 0.5100 1.000 1.400 0.900 1.400 8/3/05 0.900 0.960 0.700 0.340 0.600 0.270 0.600 0.3800 0.700 0.410 1.000 1.200 8/7/06 0.700 0.760 0.440 0.250 0.410 0.250 0.520 0.480 1.400 1.300 0.780 0.650 8/8/07 1.100 2.370 0.700 0.530 0.200 0.550 0.500 0.740 1.100 1.450 0.800 0.930 8/20/08 0.900 1.230 0.300 0.430 0.600 0.980 0.500 0.790 0.800 1.330 0.500 0.670 8/10/09 0.800 0.880 0.700 0.540 0.700 1.080 0.800 0.610 2.600 2.980 0.500 0.810 8/2/10 1.3 1.09 1.0 1.49 0.8 0.62 1.3 1.69 1.7 1.69 0.8 0.87 \) 8/23/11 0.9 1.32 0.4 0.32 0.4 0.4 0.5 0.58 1.0 1.48 0.6 0.86 8/20/12 0.5 1.96 0.4 0.54 0.7 1.09 0.6 0.81 1.6 2.70 0.8 1.37 *Data not available. EN:RGY LABORATORIES www.energylab.com Analytical ExcsJIBfiCI Sines 1952 ,Helena, MT 877·472-0711 • Billings, MT 800 .. 735-4489 • Casper, WY 888-235-0515 'qill~ti~, wY866"Q86~7175 • Rapid City, SI) 888-672-1225 • College Station, IX 888-690-2218 ANAL VTICAL SUMMARY REPORT September 21,2012 Energy Fuels Resources (USA) Inc 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C 12080965 Project Name: Annual Soils 2012 Energy Laboratories, Inc. Casper WY received the following 7 samples for Energy Fuels Resources (USA) Inc on 8/21/2012 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C12080965-001 BHV-1 08/20/128:56 08/21/12 Soil Metals by ICP/ICPMS, Total Digestion, Total Metals Digestion For RadioChemistry Radium 226 C 12080965-002 BHV-2 08/20/129:26 08/21/12 Soil Same As Above C 12080965-003 BHV-3/Black Mesa 08/20/129:47 08/21/12 Soil Same As Above C 12080965-004 BHV-4 08/20/128:20 08/21/12 Soil Same As Above C 12080965-005 BHV-5 08/20/128:32 08/21/12 Soil Same As Above C 12080965-006 BHV-6 08/20/12 8:11 08/21/12 Soil Same As Above C 12080965-007 West Water Creek 08/20/12 10:48 08/21/12 Soil Same As Above The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: cS¥~ £) tJCAi~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.09.21 13:43:29 -06:00 Page 1 of 13 www;energylab.com Analytical ExCBIIsnclI Sines '952 Helena, MT 877-412-071 t • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gilletfe,WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 CLIENT: Energy Fuels Resources (USA) Inc Project: Annual Soils 2012 Report Date: 09/21/12 Sample Delivery Group: C12080965 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. ( BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-cs -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; .Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 13 www.energylab.com EI'ERGY LABORATORIES Analytical ExcsJIBIICB Sincs 7952 Helena, MT 877-472-071 f • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~ilIe.~eJ 'NY 866-686-7175 • Rapid City, S[) 888-612-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2012 LablD: C 12080965-00 1 Client Sample ID: BHV-1 Analyses METALS -TOTAL Uranium RADIONUCLIDES Radium 226 Radium 226 precision (±) Radium 226 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 1.96 mg/kg-dry 0.5 pCi/g-dry 0.05 pCi/g-dry 0.02 pCi/g-dry MOC -Minimum detectable concentration Qualifier Rl 0.02 Report Date: 09/21/12 Collection Date: 08/20/1208:56 DateReceived: 08/21/12 Matrix: Soil MCL! QCl Method Analysis Date I By SW6020 09/20/12 11 :38 1 cp E903.0 09/17/12 21 :54 1 trs E903.0 09117/12 21 :54 1 trs E903.0 09/17/12 21 :54 1 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 13 www.energylab.com EI'iERGY LABORATORIES Analytical ExCBtJsnce S;ncs '1152 Helena, MT 877-472-0711 • Billings, MT 800-735-44B9 . Casper, WY 888-235-0515 . ~ille.t;i:eJ 'NY 866-&86-1115 • Rapid City, SD 888-&72-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2012 Lab 10: C 12080965-002 Client Sample 10: BHV-2 Analyses METALS -TOTAL Uranium RADIONUCLIDES Radium 226 Radium 226 precision (±) Radium 226 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 0.54 mg/kg-dry 0.4 pCi/g-dry 0.04 pCi/g-dry 0.02 pCi/g-dry MOC -Minimum detectable concentration Qualifier RL 0.02 Report Date: 09/21/12 Collection Date: 08/20/1209:26 DateReceived: 08/21/12 Matrix: Soil MCL! QCL Method Analysis Date / By SW6020 09/20/12 11 :42 1 cp E903.0 09117/12 21 :54 1 trs E903.0 09/17/12 21 :54 1 trs E903.0 09/17/1221 :541 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 13 www.energylab.com EI\ERGY LABORATORIES Analytical ExCSOBflCB Sincs 1952 Helena,MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 .~ille.tt¢, WY866-686-7115 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2012 Lab 10: C 12080965-003 Client Sample 10: BHV-3/Black Mesa Analyses METALS -TOTAL Uranium RADIONUCLIDES Radium 226 Radium 226 precision (±) Radium 226 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 1.09 mg/kg-dry 0.7 pCi/g-dry 0.06 pCi/g-dry 0.02 pCi/g-dry MOC -Minimum detectable concentration Qualifier Rl 0.02 Report Date: 09/21/12 Collection Date: 08/20/1209:47 DateReceived: 08/21/12 Matrix: Soil MCL! QCl Method Analysis Date 1 By SW6020 09/20/12 12:041 cp E903.0 09117/12 23:441 trs E903.0 09117/12 23:441 trs E903.0 09117/12 23:441 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 5 of 13 www.energylab.com EI\ERGY LABORATORIES Analytical ExcsllBflce Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, !NY 888-235-0515 '~illette, VlY 866-G86-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2012 Lab 10: C 12080965-004 Client Sample 10: BHV-4 Analyses METALS -TOTAL Uranium RADIONUCLIDES Radium 226 Radium 226 precision (±) Radium 226 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 0.81 mg/kg-dry 0.6 pCi/g-dry 0.05 pCi/g-dry 0.02 pCi/g-dry MOC -Minimum detectable concentration Qualifier Rl 0.02 Report Date: 09/21/12 Collection Date: 08/20/1208:20 DateReceived: 08/21/12 Matrix: Soil MCL! QCl Method Analysis Date 1 By SW6020 09/20/1212:081 cp E903.0 09/17/1223:441 trs E903.0 09117/12 23:441 trs E903.0 09117/12 23:441 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 13 www.energylab.com EN:RGY LABORATORIES Analytical ExcsJIBflCB Sines 1952 Helena, MT 871-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~illefte, WV 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2012 Lab ID: C12080965-005 Client Sample ID: BHV-5 Analyses METALS -TOTAL Uranium RADIONUCLIDES Radium 226 Radium 226 precision (±) Radium 226 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2.70 mg/kg-dry 1.6 pCi/g-dry 0.08 pCi/g-dry 0.02 pCi/g-dry MOC -Minimum detectable concentration Qualifier RL 0.02 Report Date: 09/21/12 Collection Date: 08/20/1208:32 DateReceived: 08/21/12 Matrix: Soil MCL! QCL Method Analysis Date / By SW6020 09/20/12 12:131 cp E903.0 09117/12 23:441 trs E903.0 09117/12 23:441 trs E903.0 09117/12 23:441 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 7 of 13 www.energylab.com ,EI'ERGY LABORATORIES Analytical ExcsHsncs Sines 1952 Helena, MT 877-472-0111 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 ~ille~e, WY 866-686~7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2012 Lab 10: C 12080965-006 Client Sample 10: BHV-6 Analyses METALS -TOTAL Uranium RADIONUCLIDES Radium 226 Radium 226 precision (±) Radium 226 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 1.37 mg/kg-dry 0.8 pCi/g-dry 0.06 pCi/g-dry 0.02 pCi/g-dry MOC -Minimum detectable concentration Qualifier RL 0.02 Report Date: 09/21/12 Collection Date: 08/20/1208:11 DateReceived: 08/21/12 Matrix: Soil MCL! QCL Method Analysis Date / By SW6020 09/20/12 12:17 / cp E903.0 09/17/12 23:441 trs E903.0 09/17/1223:441 trs E903.0 09/17/12 23:44/ trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 8 of 13 www.energyJab.com EN:RGY L ABORATORIES Analytical Ex~IIBflCe Sines '952 Helena, MT 877-412-0111 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY866-686-7115 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2012 LablD: C 12080965-007 Client Sample ID: West Water Creek Analyses METALS -TOTAL Uranium RADIONUCLIDES Radium 226 Radium 226 precision (±) Radium 226 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 0.08 mg/kg-dry 0.05 pCi/g-dry 0.02 pCi/g-dry 0.02 pCi/g-dry MOC -Minimum detectable concentr~tion Qualifier RL 0.02 Report Date: 09/21/12 Collection Date: 08/20/12 10:48 DateReceived: 08/21/12 Matrix: Soil MCL! QCL Method Analysis Date 1 By SW6020 09/20/12 12:21 1 cp E903.0 09/17/12 23:441 trs E903.0 09/17/12 23 :44 1 trs E903.0 09/17/1223:441 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 9 of 13 EN:RGY LABORAT ORIES www.energylab.com Analytical ExesllsncB Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WV 888-235-0515 .:~iIIette, WY866-S86-7175 • Rapid City, SO 888-672-1225 • College Station, 1)( 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2012 Analyte Count Result Units Method: E903.0 Sample 10: C120S0965-002AMS Radium 226 Sample 10: C120S0965-002AMSO Radium 226 Sample 10: LCS-34S14 Radium 226 Sample 10: MB-34S14 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: C120S0965-007AMS Radium 226 Sample Matrix Spike 1.9 pCi/g-dry Sample Matrix Spike Duplicate 1.9 pCi/g-dry Laboratory Control Sample 0.3 pCi/g-dry 3 Method Blank -0.0 pCi/g-dry 0.0 pCi/g-dry 0.0 pCi/g-dry Sample Matrix Spike 0.5 pCi/g-dry Report Date: 09/21/12 Work Order: C12080965 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: BERTHOLD 770-2_12091 OA 105 70 130 Run: BERTHOLD 770-2 120910A - 104 70 130 1.8 Run: BERTHOLD 770-2 120910A - 105 70 130 Run: BERTHOLD 770-2 120910A - Run: BERTHOLD 770-2_12091 OA 59 70 130 Batch: R164780 09/17/1221 :54 09/17/1221 :54 23.1 09/17/12 21 :54 09/17/1223:44 U 09/17/1223:44 S -Spike response and the RPD for the associated MSD are outside of the acceptance range for this analysis. Since all other QC parameters for the run are acceptable the batch is approved. Sample 10: C120S0965-007AMSO Radium 226 Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Sample Matrix Spike Duplicate 0.8 pCi/g-dry S -Spike recovery outside of advisory limits. Run: BERTHOLD 770-2_12091 OA 98 70 130 NO -Not detected at the reporting limit. R -RPD exceeds advisory limit. 46 U -Not detected at minimum detectable concentration 09/17/1223:44 26 R Page 10 of 13 E~RGY www.energylab.com G" Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 LABORATORIES Analytical Ex"llsnca Sines 1952 ~. ,~iUe~e, WY 8&6-&86-7175 • Rapid City, SD 888-672-1225 • College station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Energy Fuels Resources (USA) Inc Project: Annual Soils 2012 Report Date: 09/21/12 Work Order: C12080965 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW6020 Sample 10: ICV Uranium Sample 10: ICSA Uranium Sample 10: ICSAB Uranium Method: SW6020 Sample 10: MB-35074 Uranium Sample 10: LFB-35074 Uranium Sample 10: LCS3-35074 Uranium Sample 10: C12090561-001AOIL Uranium Sample 10: C12080965-007BMS3 Uranium Sample 10: C12080965-007BMSO Uranium Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Initial Calibration Verification Standard 0.0496 mg/L 0.00030 99 Interference Check Sample A 9.73E-05 mg/L 0.00030 Interference Check Sample AB 2.35E-05 mg/L 0.00030 Method Blank ND mg/kg 0.020 Laboratory Fortified Blank 26 mg/kg 1.0 106 Laboratory Control Sample 120 mg/kg 1.0 119 Serial Dilution 13 mg/kg-dry 1.0 Sample Matrix Spike 25.5 mg/kg 1.0 103 Sample Matrix Spike Duplicate 25.8 mg/kg 1.0 103 Analytical Run: ICPMS4-C_120919A 09/19/12 13:55 90 110 Run: ICPMS4-C_120919A Run: ICPMS4-C_120919A 80 120 Run: ICPMS4-C 120919A - 80 120 Run: ICPMS4-C 120919A - Run: ICPMS4-C_120919A 75 125 Run: ICPMS4-C_120919A 75 125 11 1.1 09/19/12 13:59 09/19/12 14:04 Batch: 35074 09/20/12 11 :08 09/20/12 11 :13 09/20/12 11 :17 09/20/12 11 :29 10 R 09/20/12 12:26 09/20/12 12:30 20 ND -Not detected at the reporting limit. R -RPD exceeds advisory limit. Page 11 of 13 \ EI'£RGY LABORATORIES ~JNwww.energylab.com ~ Analytical Excs/lsnce Sines 1852 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 .§ille!t~, Wy ~66~686-7175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Energy Fue ls Resources (U SA) Inc Login completed by: Timothy I.. Houghteling Reviewed by: BL2000\kschroeder Reviewed Date: 8/24/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Temp Blank received? ContaineriTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes III Yes III Yes D Yes III Yes III Yes III Yes III Yes III Yes III Yes III Yes D N/A"C Yes D Yes D C12080965 Date Received: 8/21/2012 Received by: km Carrier Ground name: No D No D No D No D No D No D No D No D No D No D No D No D No D Not Present D Not Present D Not Present III Not Applicable III No VOA vials submitted III Not Applicable III Page 12 of 13 "U Q) co CD ~ w o -w EN:RGY .-Chain of Custody and Analytical Request Record Page ---1-of --\--. -_ ... --......... ....1.. •• ,.. •• -.... --....... "'fP .................................. ~ ..,"W'"....,."W' ..... ...,..., Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPAfState Compliance: , I ;: v\.Lr-c. \.1 ~l)e\~ A ~lI\u c..., \ ~oll.s :1012 State: VI Yes g No 0 Report Mail Address: -.J I Contact Name: Phone/Fax: Email: Sampler: (Please Print) Ro. £,,)1: go q ?~f"',..;,r..... P~lAAe.r t..j'3S 67 t z~;al Hol\'.J..A'/ JSIA.~;M uY rt.i5tl '-~"'-"'e...r- I nvoice Address: "-"" . Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: S /)""V"'" e-SC-~t:.. ,Lt-tYl. Special Report/Formats: 3: ~W~O~ OO[3@)U1J~[Q) ... Contact ELI prior to ~uffi~~~ 0 '"'-RUSH sample submittal ~O(l)~ ~ R for charges and Cooler IO(Sl: ~CQ~OI ~ 0 scheduling -See ._> 0 :>..(6 W t:. Instruction Page r\~p.1\Y · DDW o EDD/EDT(Electronic Data) ~en~ m 3: 0:;::= fQ 0") J: "0 Receipt Temp o POlWIWWTP C,.) c: Comments: Format: ~<cc55l.2 ~ ::J U' lJlA: o ,-COl c: « a °c o State: D LEVEL IV I-'-QiS c: or.: I-ro --~ o.aJrg 0 '-C ~ c: Y~ D Other: D NELAC E~(Q , :s On Ice: ::J .!? :a:1 Q) s: ~ + i-S Z c.. 010 { W 'E Custody Seal ~<r E ~I W m On Bottle aJ C/) "0 en c: On Cooler ~ CO :0 j Ci5 H Intact SAMPLE IDENTIFICATION Collection Collection ~ """'" MATRIX ...... Signature (Name, Location, Interval, etc.) Date Time Match 1 ISH-v-I R/-;u,J i ;;. OH-"~b ,.-S ~ )t I~ 2 EHV -.2 ( -~ OQ2b ) -S -y: y: 3 B H-tJ -.3 I Ele....c.J<-A.A •. "'" OQ'-i7 l ... .s ~ .. .)(. ~ nnn 4 E H--V-Y _0 f'U) l-5 x: X I 5 &~ 1I-5 ( Oi32. I -.$ 1..:::;/ X x: ~ 6E~v' -~ 1J~1I J -S )( ~ ~~I 2..of(cIi'J 7 Wt....S.l.lj&o..t ~r ~ Z"'I" \( fl~lil \01.-/8 \ -s X " ~ 8 ~ 9 .~ ~ 10 .J] Custody Relinquished by (print): Datemme: Signature: Received by (print): DatefTime: Signaure: G().rr-\A. PA\"""',u-., 2.oiJ 2. / j -:JDo &~ PJAA. Record Relinquished by (print): Datemme: Signature: Received by (print): DatelTime: Signature: MUST be Signed 1~~YiVfiJJj~ ua~t~\I\d ~lD ::JlgnaIUre: Sample Disposal: Return to Client: Lab Disposal: . In certain circumstances. samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract dam-wlli be clearly notated on your analytical report. ..... -. • -. ~ • -I. __ .• -~ _ .• _..J ..J~j.~ ___ -.1 :_.t' _____ :--": __ .... _ .... _1 __ ... _"'-1_ ~ .... ,... A I"'Ioh ""A a .. I~ f"' .. ....,~ "3""" ti .... l.te