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DRC-2012-001788 - 0901a0688030017d
DRC-2012-001788 Energy FUEIS Resources IU5R1 Inc. August 22, 2012 VIA OVERNIGHT DELIVERY Mr Rusty Lundberg Director of the Utah Division of Radiation Control State of Utah Department of Environmental Quality 195 North 1950 West P O Box 144850 Salt Lake City, UT 84116-4850 Dear Mr Lundberg Re: State of Utah Radioactive Material License No. UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period January 1,2012 through June 30,2012 As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40 65 (subpartl)), and License Condition 11 3A of State of Utah Radioactive Matenals License No UT 1900479, enclosed is the Semi-Annual Effluent Monitonng Report for the White Mesa Mill for the period January 1, 2012 through June 30, 2012 If you have any questions regarding this report, please contact the undersigned at (303) 389- 4132 Yours f -,^.,.oONMINES (USA) CORP. lA--JO Ann Tischler Director, Compliance cc Harold R Roberts David C Frydenlund David E Turk Kathenne A Wemel August 22, 2012 VIA OVERNIGHT DELIVERY Mr. Rusty Lundberg Director of the Utah Division of Radiation Control State of Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144850 Salt Lake City, UT 84116-4850 Dear Mr. Lundberg: Re: State of Utah Radioactive Material License No. UT1900479 White Mesa Mill, Blanding, Utah Semi-Annual Effluent Monitoring Report for Period January 1,2012 through June 30, 2012 As required by Utah Administrative Code, R 313-24-4 (incorporating by reference 10 CFR 40.65 (subpart 1)), and License Condition 11.3A of State of Utah Radioactive Materials License No. UT1900479, enclosed is the Semi-Annual Effluent Monitoring Report for the White Mesa Mill for the period January 1, 2012 through June 30, 2012. If you have any questions regarding this report, please contact the undersigned at (303) 389- 4132. SON INES (USA) CORP. Fvt---JoAnn Tischler Director, Compliance cc Harold R. Roberts David C. Frydenlund David E. Turk Katherine A. Weinel Eneq;y Fuels Resources (USA) 1nc. Lakewood, CO 80228 225 Union Boulevard, Suite 600 Phone: 303-974-2140 White Mesa Uranium Mill Radioactive Materials License UT900479 Semi-Annual Effluent Monitoring Report (January to June 2012) Prepared For: Utah Department of Environmental Quality Division of Radiation Control Prepared by: Energy Fuels Resources (USA) Inc. Formerly Denison Mines (USA) Corp. 225 Union Boulevard, Suite 600 Lakewood, CO 80228 August 22, 2012 Table of Contents 1.0 IN"TRODUCTION .................................................................................................. 1 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLIN"G ..................................... 2 2.1 Program Overview ............................................................................................... 2 2.2 Sampling Protocol and Analytical Results ........................................................... 2 2.3 General Observations ........................................................................................... 3 2.4 Site Specific Sampling Data ................................................................................. 4 2.5 Radon-222 ............................................................................................................ 6 3.0 EXTERNAL RADIATION (DIRECT GAMMA) .................................................. 7 4.0 VEGETATION SAMPLES ..................................................................................... 8 5.0 STACK SAMPLIN"G ............................................................................................... 8 6.0 SURFACE WATER MONITORIN"G .................................................................... 11 7.0 SOILSAMPLIN"G ................................................................................................. 11 8.0 METEOROLOGICAL MONITORIN"G ................................................................ 11 9.0 SIGNATURE ......................................................................................................... 12 LIST OF TABLES Table 1 NCRP Report 94-Global Pb-210 Concentration Example Table 2 Air Monitoring Station Results U-Nat (Comparison to Limits) Table 3 Air Monitoring Station Results Th-230 (Comparison to Limits) Table 4 Air Monitoring Station Results Ra-226 (Comparison to Limits) Table 5 Air Monitoring Station Results Pb-210 (Comparison to Limits) Table 6 Environmental OSL Dosimeter Measurements (Gamma) Table 7 Stack Sampling Requirements Table 8 Stack Effluent Concentrations and Release Rates i INDEX OF TABS A High Volume Air Monitoring Stations B BHV Air Sampling Graphs and Data Tables Tabl BHV-l Air Sampling Graphs and Data Table Tab 2 BHV -2 Air Sampling Graphs and Data Table Tab 3 BHV -3 Air Sampling Graphs and Data Table Tab 4 BHV -4 Air Sampling Graphs and Data Table Tab 5 BHV -5 Air Sampling Graphs and Data Table Tab 6 BHV -6 Air Sampling Graphs and Data Table C Air Particulate Loading Graphs and QAlQC D Air Particulate Loading Graphs and Supporting Data E Environmental Gamma (OSL) Dosimeter Graphs and Supporting Data F Vegetation Graphs, Data Table, Laboratory Results and QAlQC G Stack Sample Laboratory Results H Surface Water Graphs and Field Data Sheets I Soil Sample Graphs, Data Table, Laboratory Results and QAlQC 11 WHITE MESA URANIUM MILL SEMI-ANNUAL EFFLUENT REPORT, JANUARY THROUGH JUNE, 2012 1.0 INTRODUCTION The White Mesa Mill (the "Mill") has established monitoring programs to evaluate compliance with effluent limitations and to assess the potential for release of radioactive material into the local environment. These monitoring programs were developed and implemented at the time of Mill construction, operated with appropriate adaptation over time, and are consistent with the Mill's State of Utah Radioactive Materials License No. UT1900479 (the "License") and guidelines developed by the United States Nuclear Regulatory Commission ("NRC") (NRC Regulatory Guide 4.14, Radiological Effluent and Environmental Monitoring at Uranium Mills-Rev. 1, ML003739941), 1980). Under these programs, the Mill monitors the following environmental media and conditions: a) Airborne particulate radionuclide concentrations obtained from the following sampling stations: • North, east and south of the Mill Site: BHV-1 and BHV-2 (north), BHV-5 (east), and BHV-4 (south). BHV-1 serves as a surrogate for the nearest resident (BHV -1 is approximately 1.2 miles north of the Mill, but approximately 0.4 miles closer to the Mill than the nearest resident); • A background location distant to and west of the Mill (BHV-3), which was monitored for airborne particulate up until November, 1995, at which time background was established, but is no longer monitored for air particulate; and • A station specifically requested by the White Mesa Ute Community south of the Mill Site (BVH-6); a) External (direct) gamma radiation measured at air monitoring stations BHV-1, BHV-2, BHV-3, BHV-4, BHV-5 and BHV-6; b) Vegetation at three site periphery locations, for uptake of radiation; c) Stack release rates from the Mill's air emissions sources; d) Surface water at Cottonwood Creek and, when flowing, Westwater Creek, both located west of the Mill; e) Soil radionuclide activity obtained near the air particulate monitoring stations, during the third quarter of each year; 1 N:\Required Reports\Semi Annual Effluent Reports\2012 Jan to June\Jan_to_June_2012_SAER_text.docx f) Groundwater (up and down gradient) of the Mill facility; and1 g) Seeps and springs in the vicinity of the Mill.l This semi-annual effluent report provides the results of the specific monitoring and sampling activities that were undertaken during the subject reporting period. 2.0 ENVIRONMENTAL AIR PARTICULATE SAMPLING 2.1 Program Overview The environmental airborne particulate monitoring program at the Mill utilizes four air sampling stations. Four high-volume continuous air sampling stations (BHV-l, BHV-2, BHV -4, and BHV -5) are required by the License. These sampling stations serve as sentinels for airborne particulate which could potentially emanate from the Mill site. In addition to its general site monitoring function, BHV -1 also serves as a conservative surrogate for concentrations at the nearest resident, because it is located approximately 1.2 miles north of the Mill just south of the nearest resident but between the Mill and that resident. With regard to background monitoring, the Mill previously operated a continuous high- volume air sampling station (BHV-3) which was located approximately 3.5 miles west of the Mill site. With the approval of NRC, this station (BHV-3) was removed from the active air monitoring program in November 1995. At that time, NRC determined that a sufficient air monitoring data base had been compiled at BHV-3 to establish a representative airborne radionuclide background for the Mill. It should be noted, however, that while air sampling was discontinued at this location, gamma measurements and soil sampling continue to be collected at BHV -3. In addition to the environmental air sampling locations described above, an additional station (BHV -6) was installed at the request of the White Mesa Ute Community. This station began operation in July of 1999 and provides airborne particulate information in the southerly direction between the Mill and the White Mesa Ute Community 2.2 Sampling Protocol and Analytical Results Airborne particulate monitors are operated continuously at each of the high-volume air sampling stations referenced above except BHV -3, as noted above. Particulate sample collection filters are gathered by site technicians weekly in accordance with the Mill's environmental air sampling procedures and are composited on a quarterly basis for laboratory analyses. The collected filters are analyzed for Unat activity, Th-230 activity, Ra-226 activity, and Pb-210 activity. Fugitive dust standards for the facility are limited by the Mill's State of Utah Air Approval Order, which sets a 20% visual opacity 1 Groundwater sampling and seeps and springs sampling are reported separately pursuant to the Mill's State of Utah Ground Water Discharge Permit No. UGW370004, and are not included with this report. 2 N:\Required Reports\Semi Annual Effluent Reports\2012 Jan to June\Jan_to_June_2012_SAER_text.docx standard. The specific locations of the Mill's airborne particulate monitoring stations are depicted on the figure entitled High Volume Air Monitoring Stations included as Attachment A. Station BHV-3, which is no longer sampled for air particulate, is located approximately 3.5 miles west of the Mill facility and is not indicated on that Figure. The analytical results of radionuclide particulate sampling for each monitoring station operated during this reporting period are provided in Attachment B under separate sampling station attachment tabs (Tabs 1-6). Each Tab contains graphical illustrations of the radionuclide concentrations in log-scale presentation format. The graphs display reported data over time since the 1981 inception of the Mill's environmental air particulate monitoring program. The actual analytical results (and associated QAlQC information) reported by the laboratory for the reporting period are provided under Attachment C. In addition to the analyses for radionuclides, particulate loading is determined for each filter and compo sited as a quarterly mass-loading estimate for review purposes only. Graphs showing particulate loading at each station for the first half of 2012 and the underlying data are included as Attachment D. It should be noted that for BHV-6 the first 2 sampling periods of April 2012 have been omitted from particulate loading on the graph in Attachment D. The timer on the airborne particulate monitoring station at BHV -6 malfunctioned and the data are considered invalid due to the inability to measure the time sampled. The timer was replaced prior to the third sampling period and all other measurements are valid. It should be noted that for graphical illustration purposes, values reported at zero, values reported at less than the prescribed detection limit « 1 X 10-16 uCi/ml) and missing values were plotted as 1 x 10-16 uCi/ml concentrations. Where other "less than" values were indicated (i.e., where detection limits for the data varied from 1 x 10-16 uCi/ml), the detection limit concentration was utilized for plotting the data point. This graphing convention is not utilized to formulate station average information, nor is it intended as a precedent for data treatment. Rather, the intent is to provide a conservative viewable depiction of site airborne radionuclide information. This is considered to be a conservative approach because the actual concentration below the detection limit cannot be determined and, as a result, the plotted point will be at the same or a higher concentration than the actual activity concentration of the collected sample. 2.3 General Observations The results of environmental air monitoring for this semi-annual period indicate that for all radionuclides at all monitoring stations airborne radionuclide particulate activity concentrations were well below regulatory Effluent Concentration Limits ("ECL's") and the Mill's ALARA goals, which are set at 25% of the ECLs. It is noteworthy and expected that Pb-210 concentrations are elevated when compared to the other parent radionuclide concentrations (i.e. U-nat, Th-230 and Ra-226). This phenomenon is due to the well-established controlling effect experienced worldwide as a 3 N:\Required Reports\Serni Annual Effluent Reports\2012 Jan to June\Jan_to_June_2012_SAER_text.docx result of the ubiquitous presence of radon in the earth's atmosphere. Accordingly, elevated Pb-210 presence in disequilibrium with parent radionuclides measured here is not associated with uranium milling operations. Rn-222 emanates as a decay-chain progeny of the Ra-226 contained in the soil of the earth's crust and is dispersed generally throughout the earth's atmosphere. The electrically charged short and long-lived decay products of Rn-222 attach to ambient dust particles found naturally in the atmosphere and are carried with the air. Pb-210 is the longest lived of these decay products and is the decay product of the shorter-lived radon progeny. As such, it accumulates as an electrical attachment on the natural ambient dust in the atmosphere and is generally measured at elevated activity when compared to local decay-chain parent radionuclide activity, regardless of uranium milling activity. At the Mill's BHV air monitoring stations, all dust (ambient natural and mill derived) is collected by the sample filter. Because of the natural elevation of Pb-210 accumulated as an attachment to the naturally occurring ambient dust particles collected by the air sampling equipment, Pb-210 is commonly elevated and in disequilibrium when compared to parent radionuclide activity, regardless of the Mill's presence. By way of illustration, average ground-level concentrations have been reported for selected States (NCRP Report 94, 1992) and are summarized in Table 1 below, demonstrating elevated Pb-210 activity where no uranium milling operations are located nearby. Pb-210 activity concentrations can be expected to be even higher for locations in the western U.S. where uranium ore bodies are commonly located. In April 1977, prior to Mill construction and Mill operations, air particulate Pb-210 was measured at the Mill site to be 1.3E-14 uCi/ml (l3.0E-3 pCi/m3)2 Table 1-NCRP Report 94-Global Pb-210 Concentration Example State .~ ·Ph-210 Concentration ., , , " "K' " UB.g~3i . uCi/ml ·'f.· . ..; .,,.. :' c.:. '.' '" ',' c' J! . , . California 600 1.6E-14 Illinois 1500 4.1E-14 Ohio 300 8.1E-15 Massachusetts 700 1.9E-14 2.4 Site Specific Sampling Data The results of airborne particulate monitoring for the period (without background subtraction) are provided by sampling station and radionuclide in Tables 2 through 5 below. Along with these data, the tables present comparative ECL's and the ECL percentage measured at each of the monitoring stations sampled during the period. A review of these data supports the conclusion that airborne particulate is well controlled at the Mill. In all cases, the measured activity concentrations were well within the ECL, as well as the Mill's ALARA goal (i.e. 25% of the ECL). Lower Limits of Detection 2 See the Environmental Report, White Mesa Uranium Project, San Juan County, Utah for Energy Fuels Nuclear, Inc. prepared by Dames & Moore, January 30,1978, Section 2.9.1.1 4 N:\Required Reports\Semi Annual Effluent Reports\2012 Jan to June\Jan_to_June_2012_SAER_text.docx consistent with NRC Regulatory Guide 4.14 were maintained by the Mill's contract analytical laboratory for this reporting period. In fact, the data obtained since program inception in 1981 indicates that only one individual quarterly measurement (Th-230 at BHV-5 for the 2nd Quarter of 1996) has ever exceeded the ECL at the Mill. With regard to that particular single measurement, while it is important to consider and evaluate an individual measurement exceeding the ECL, for public dose estimation purposes, it is the average annual concentration that is of primary significance. In that instance, the average annual concentration of Th-230 for BHV -5 in 1996 was well below the ECL. Data obtained since program inception in 1981 also indicate that, with very few exceptions, the gross (background inclusive) measurements do not exceed the site's ALAR A goal (i.e. only nine of the several thousand total gross radionuclide determinations to date exceeded the Mill's self-imposed 25% ALARA goal). Table 2-Air Monitoring Station Results U-Nat (Comparison to Limits) 1st and 2nd Quarters 2012 MonitorinK 1st Qtr. 2nd · tr. .; Q Effluent Average Statiori Result Result ;;, ~(Jonpentration ' Percent .. { ,(uei/ml) ',' (uCi/ml) I:,imit (ECL) I~~', E~L" , ". , ": '." 0.; ",_ ,s . , ',,: « .... ,. ,f' . , '0 ''',;" ' t ,(uCiJrnl) " '~. !l' ., BHV1 7.87E-16 1.86E-15 9.00E-14 1.47E+OO BHV2 4.22E-16 3.39E-16 9.00E-14 4.23E-01 BHV4 2.51E-15 2.62E-15 9.00E-14 2.85E+OO BHV5 5.52E-15 5.87E-15 9.00E-14 6.33E+OO BHV6 4.41E-15 6.42E-15 9.00E-14 6.02E+OO Table 3-Air Monitoring Station Results Th-230 (Comparison to Limits) 1st and 2nd Quarters 2012 Monitoring . 1st ,Qtr. 2nd Qtr.· '"' " Effluent I' Average , ' . Station Result . Result ., Concentration Bercent I· i (uCi/ml) ., (uCi/:ml) . Limit (ECL) '. _"ECL, ". :\.i.,':;-;,,};-; , .X ' " .' '";~;,, ,:.' ' <. :; (ti€iJinl) .. "Y'): :i'::e;' BHV1 2.64E-16 8.33E-16 2.00E-14 2.74E+OO BHV2 1.15E-16 1.56E-16 2.00E-14 6.78E-01 BHV4 5.02E-16 1.23E-15 2.00E-14 4.33E+OO BHV5 3.24E-15 3.06E-15 2.00E-14 1.58E+01 BHV6 1.82E-15 2.25E-15 2.00E-14 1.02E+01 5 N:\Required Reports\Semi Annual Effluent Reports\2012 Jan to June\Jan_to_June_2012_SAER_text.docx Table 4-Air Monitoring Station Results Ra-226 (Comparison to Limits) 1st and 2nd Quarters 2012 BHVI 3.95E-16 9.85E-16 7.67E-02 BHV2 2.77E-16 1.74E-16 9.00E-13 2.S1E-02 BHV4 2.27E-16 2.97E-16 9.00E-13 2.91E-02 BHVS 1.79E-15 1.21E-15 9.00E-13 1.67E-Ol BHV6 4.00E-16 5.11E-16 9.00E-13 S.06E-02 Table 5-Air Monitoring Station Results Pb-210 (Comparison to Limits) 1st and 2nd Quarters 2012 Monitoring 1st Qtr.. 2nd Qtr. " .·Effluent · Average I" Station ,: Re~u.lt . Result 'Concentration . Percent ,;. . (uCi/mi}~ . .' .. ,(uCi/nil) . ".L--imit (ECL) .:' Eel.,' , .. ',It, , .'l.., ~ , . . '<::,: . . (uei/nil) T' ~ , I C' ". , '''0; BHVI 1.25E-14 9.55E-15 6.00E-13 1.84E+OO BHV2 1.58E-14 8.60E-15 6.00E-13 2.03E+OO BHV4 1.03E-14 9.27E-15 6.00E-13 1.63E+OO BHVS 1.55E-14 1.11E-14 6.00E-13 2.22E+OO BHV6 1.50E-14 9.54E-15 6.00E-13 2.0SE+OO 2.5 Radon-222 Due to the unavailability of monitoring equipment to detect the revised 10 CFR Part 20 standard, and with the approval of NRC, Radon 222 monitoring at BHV stations was discontinued in 1995. Instead, Denison demonstrates compliance with these limits and the requirements of R313-15-301 by calculation, authorized by the NRC and as contemplated by R313-15-302(2)(a). A copy of the Technical Evaluation Report evidencing such approval was enclosed with correspondence to the Division of Radiation Control ("DRC") on July 28, 2008. This calculation is performed by use of the MILDOS code for estimating environmental radiation doses for uranium recovery operations (Strenge and Bender 1981) and more recently in 2003 by use of the updated MILDOS AREA code (Argonne 1998). The. analysis under both the MILDOS and MILDOS AREA codes assumes the Mill to be processing high grade Arizona Strip ores at full capacity, and calculates the concentrations of radioactive dust and radon at individual receptor locations around the Mill. 6 N:\Required Reports\Semi Annual Effluent Reports\2012 Jan to June\Jan_to_June_2012_SAER_text.docx The MILDOS and MILDOS AREA codes calculate the combined Total Effective Dose Equivalent ("TEDE") from all relevant pathways, including both air particulate and radon, at a number of locations including the nearest residence (the individual likely to receive the highest dose from the licensed operation), approximately 1.6 miles north of the Mill. These calculations reveal projected doses to the individual likely to receive the highest dose from the licensed operations to be well below the 1 00 mrem regulatory limit in R313-15-301(1)(a) for all pathways, including air particulate and radon, and well below the ALARA goal of 10 mrem/yr for air emissions excluding radon as set out in R313-15-101(4). MILDOS AREA modeling was recently conducted in support of the Mill's 2007 License Renewal Application, utilizing the MILDOS-AREA code (Version 2.20~), to estimate the dose commitments at various receptor locations for processing of Colorado Plateau ore (0.25% U30 8 and 1.5% V 205) and Arizona Strip ore (0.637% U30 8). The process rate was assumed to be at full capacity of 730,000 tons per year (an average of 2,000 tons per day) with an average uranium recovery yield of 94%. That modeling showed a TEDE of 2 mrem per year at the nearest resident (3 mrem per year at the nearest potential residence, being the location of BHV -1 at the northern property boundary of the Mill site), which included the dose from all radionuclide sources, including radon. The modeled dose from radon itself was therefore a fraction of TEDE and well within the regulatory limits. 3.0 EXTERNAL RADIATION (DIRECT GAMMA) Gamma exposure rate estimates were measured for the reporting period utilizing passive integrating devices, optically stimulated luminescence dosimeters ("OSLs"). These dosimeters were located at each of the Mill's high-volume air sampling stations (BHV -1, BHV-2, BHV-4, BHV-5 and BHV-6) and at the designated background monitoring station (BHV-3). Measurements obtained from location BHV-3 have been designated as background due to BHV-3's remoteness from the Mill site (i.e. BHV-3 is located approximately 3.5 miles west of the Mill site). The results of the environmental OSL measurements and semi-annual cumulative above-background data are provided in Table 6 below. In addition, measurement data obtained at these locations are graphically presented at Attachment E to this report. 7 N:\Required Reports\Semi Annual Effluent Reports\2012 Jan to June\Jan_to_June_2012_SAER_text.docx Table 6-Environmental Optically Stimulated Luminescence Dosimeter ~easurements (;amma) Monltoriilg . '1st Qtr 2nd .. Qtr · 1st Qtr " 2nd·Qtf. C~mulative Station ' , Result ' .Resu,lt Result Less Result Less s~nri> '" .:(mrem) ',' Il.BaCkground ~, ,(ntrem) . Background, , .Annual , : I: " (mrem) " :' ~ (mrem) :; Estitp.at,e * ,.,''1;' 'I" :, " > .;) (IIlfe,m) i , ' ;' f: ." '. ,.1<, \ ';'.,,, .. ' ;,' I':''''' ..... .;: BHV1 33.2 38.6 4 7.5 11.5 BHV2 28.9 31.6 -0.3 0.5 0.2 BHV3 29.2 31.1 0 0 0 BHV4 30.6 35.1 1.4 4 5.4 BHV5 33.4 37.5 4.2 6.4 10.6 BHV6 30.3 32.6 1.1 1.5 2.6 *Negative values treated as zero for cumulative dose The results for this period indicate that above background measurements for stations BVH-l, BVH-2, BVH-4, BVH-S and BHV-6 are within regulatory limits. BHV-l is at the location of the nearest potential residence. The nearest actual residence is approximately 0.4 miles north of BHV -1. The annual individual member of the public limit is 100 mrem/yr for combined internal and external exposure. 4.0 VE(;ETATION SA~PLES Vegetation samples are collected at three locations around the Mill property. The sampling locations are: 1) northeast, 2) northwest and 3) southwest of the Mill facility. The U.S. Nuclear Regulatory Commission ("NRC") Regulatory Guide 4.14 requires that three samples be collected during the grazing season, without specifying exact months or times during the season. During the 2012 grazing season, two sets of samples have been collected, on April 11, 2012, and June 11, 2012. A third set of samples is planned for the fall season. At the conclusion of the third quarter of 2011, three sets of samples have been collected consistent with Regulatory Guide 4.14. The data from the fall season sampling will be included in the July through December 2012 Semi-Annual Effluent Report ("SAER") which was submitted to the DRC on March 1,2013. Data from the April and June sampling events are included in this report. Graphical log-scale presentation of the vegetation sampling results, together with the analytical results reported by the Mill's contract laboratory (including QAlQC information) for this sampling period, are included at Attachment F of this report. The 2011 data results are within the variation of previous sampling episodes. 5.0 STACKSA~PLIN(; Under Section S.O of Tab 1.4 of the Mill's Environmental Protection Manual, Revision: DUSA-l, 2/07 (the "Environmental Protection Manual") gas stack samples are collected 8 N:\Required Reports\Semi Annual Effluent Reports\2012 Jan to June\Jan_to_June_2012_SAER_text.docx at the Mill in accordance with the calendar year schedule shown below: Table 7 -Stack Sampling Requirements Frequency Feed Stack (Grizzly Stack for Packaging Baghouse) Yellowcake Dryer (Yellowcake Baghouse) Quarterly None If operating, V-nat If operating, V-nat Semi -annuall y If operating, V-nat, If operating, V-nat, If operating, V-nat, Th-230 Th-230, Ra-226, Pb-Th-230, Ra-226, 210 Pb-210 The yellowcake dryer and yellowcake baghouse operated during the 1 st and 2nd quarters of 2012. During the first half of 2012, the main Mill circuit did not operate. During the second quarter of 2012, the main Mill circuit processed alternate feeds. Therefore the grizzly baghouse was not in use either quarter, and no gas stack samples were collected during the 2nd quarter of 2012. The analytical results of stack sampling conducted for the 3rd and 4th quarters of 2011 and for the 1 st and 2nd quarters of 2012, are provided in Table 8 below, indicating the uCi/cc concentration in the stack emissions and the stack's radionuc1ide release rate (uCi/sec) for V-Nat, Th-230, Ra-226 and Pb-210 at each of the stacks sampled. The actual analytical results reported by the laboratory for the 1 st and 2nd quarters of 2012 are provided in Attachment G to this report. It is also important to note that stack effluent concentrations are not comparable to environmental air sampling station ECL's for regulatory compliance purposes. The ECL is a limit that applies to the receptor locations and is not applicable to effluents from mill processes on the Mill site. These stack release data are more appropriately utilized for dose modeling purposes, and dose modeling is not computed for semi -annual reporting purposes. 9 N:\Required Reports\Semi Annual Effluent Reports\2012 Jan to June\Jan_to_June_2012_SAER_text.docx Table 8-Stack Effluent Concentrations and Release Rates Dryer, Run 1 No samples were Required Required North YC collected as the facility Not Not Dryer, Run 2 was not operating due Required to a maintenance Yellowcake shutdown. Not Not North YC 6.02E-12 3.S2E-06 2.96E-13 1.74E-07 7.4SE-14 4.36E-OS 3.91E-12 2.29E-06 Dryer, Run 1 North YC S.29E-09 4.74E-03 7.76E-13 4.43E-07 S.S3E-14 3.16E-OS S.00E-12 2.SSE-06 Dryer, Run 2 Yellowcake 1.0SE-09 1.17E-03 4.0SE-13 4.3SE-07 3.99E-14 4.31E-OS 1.9SE-13 2. 14E-07 6.73E-12 3.S1E-06 1.47E-13 Dryer, Run 1 9.71E-09 North YC 1.27E-OS 7.S3E-03 Dryer, Run 2 Yellowcake 6.33E-10 6.2SE-04 North YC 1.12E-OS S.60E-03 l.S4E-13 7.72E-OS 1.37E-14 6.S4E-09 3.2SE-12 1.63E-06 Dryer, Run 1 North YC 1.13E-08 6.7SE-03 2.4SE-12 1.47E-06 2.13E-14 1.2SE-OS 2.27E-12 1.36E-06 Dryer, Run 2 Yellowcake 3.04E-09 3.32E-03 1.1SE-ll 1.2SE-OS 7.S0E-14 S.SOE-OS 3.64E-13 3.97E-07 Baghouse Grizzly *Not *Not *Not *Not Baghouse Running Running Running Running * Grizzl y B aghouse was not operating during the 1 st or 2nd quarter of 2012, because the Mill's alternate feed circuit was running and no ore was being grinded. 10 N:\Required Reports\Semi Annual Effluent Reports\2012 Jan to June\Jan_to_June_2012_SAER_text.docx 6.0 SURFACE WATER MONITORING Under the License, Part 11.2 B surface water samples are required to be obtained annually from Westwater Canyon and semi-annually from Cottonwood Creek. Sediment samples from Westwater Canyon are taken in place of the Westwater Canyon surface water sample in the event that surface water is not available for sampling. Westwater Canyon surface water was not sampled in the first or second quarter 2012 because no water was present during this reporting period. Attempts to collect a surface water sample from Westwater Canyon will continue through the next reporting period. If no surface water is available, a sediment sample will be collected as required. The Mill's Environmental Protection Manual, requires that Cottonwood Creek be sampled for TDS and total suspended solids TSS quarterly, and the License, Part 11.2 B requires that Cottonwood Creek be sampled for dissolved and suspended radionuclides including Gross Alpha, Unat, Ra-226, Th-230 semi-annually. In accordance with these requirements, Cottonwood Creek was sampled for TDS and TSS durin§ the 1st quarter. Surface water was not collected from Cottonwood Creek during the 2n quarter of 2012 because there was no surface water present during the quarter. The field data sheets for the surface water sampling events, along with graphs showing historic results are included as Attachment H. The results of this sampling indicate that surface water results remain low and within the range of typical background. 7.0 SOIL SAMPLING Under Tab 4.1 of the Mill's Environmental Protection Manual, surface soils are required to be sampled at the Mill's air monitoring stations (BHV-1, BHV-2, BHV-3, BHV-4, BHV -5 and BHV -6) once per year during August or as soon as possible thereafter, but no later than -September 30 of each year. In accordance with the Mill's Environmental Protection Manual, surface soils will be collected during the third quarter 2012 and will be discussed in the July through December 2012 report. 8.0 METEOROLOGICAL MONITORING As in prior reporting periods, an independent contractor has prepared the White Mesa Mill Semi-annual Meteorological Monitoring Report for the period of January through June, 2012. This information is retained at the Mill site for agency review. 11 N:\Required Reports\Semi Annual Effluent Reports\2012 Jan to June\Jan_to_June_2012_SAER_text.docx 9.0 SIGNATURE This Report was prepared by Energy Fuels Resources (USA) Inc. on August 22, 2012. Energy Fuels Resources (USA) Inc. By: Dav· C. Fry nlund Senior Vice President, Regulatory Affairs and General Counsel 12 N:\Required Reports\Semi Annual Effluent Reports\2012 Jan to June\Jan_to_June_2012_SAER_text.docx ATTACHMENT A HIGH VOLUME AIR MONITORING STATIONS W.\USA\Ulill'l~~\qfl:clamaIlClll~3.2·ttlllll\!o~e~~L~~~lOtI'!!1,~AgwIt~~l 14101trol' ~IU1baG!lIr ~ ____ ~~~+~~~~---+------~--+-r----------~ ~ C I • ."..-J .. I ~ / : ... ~. I N I w , ... V ':. . V \ \ \ t\;",:~~1.-.. ~ \ !01 ... '1: , \ A i + \ , l' / /1 I i I . \ ~/-l'! \ I L,--. ~ ~. . ~ .. _-----.-J ~ _/ t .... I _II .L_ -! ~_ r ~ _'" __ .---._i_ ~ r---''-':: : ~ " .... '\. '\ ""'-". '----;, ! \ t, ... ·1' ;". ". ~f' .. ;, _n_u r". ~.. -, l\ ......... ~,k I I ~ ..... ;. I'l ... ..,-... ... I ~ ~~ 1/ ( , J Denison Mines (USA) Corp. Property Boundary Reservation Boundary Canyon Rim o Air Monitor Stations Project WHITE MESA MILL REVISIONS I County: SAN JUAN Stale: UT Dale J ~ I Loi:aliol'l; Figure 2.3-1 High Volume Air Monitoring Stations (KNLSOHI);~ .,m.s I ScalE!: n~.~ I Date: JAN 2011 lfigure 2.3-L.olr monitGtinl'cfW; AUthor: HRR I DriiJicij'sy; B. IIunkhbaotar ATTACHMENT B BHV AIR SAMPLING GRAPHS AND DATA TABLES TAB 1 BHV-l AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-lU Effluent Concentration Limit = 2E-14 uCi/ml BHV-lT Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = 6E-13 uCi/ml BHV-1PB ALARAGoal = 2.2SE-14 uCi/ml ALARA Goal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 2.35E-15 5.00E-12 1.25E-12 7.82E-16 8.00E-14 2.00E-14 1.06E-15 2.00E-12 5.00E-13 2.57E-14 4.00E-12 1.00E-12 12/14/1981 1.56E-15 5.00E-12 1.25E-12 1.49E-15 8.00E-14 2.00E-14 1.93E-15 2.00E-12 5.00E-13 2.64E-14 4.00E-12 1.00E-12 3/29/1982 2.16E-15 5.00E-12 1.25E-12 2.93E-15 8.00E-14 2.00E-14 1.16E-15 2.00E-12 5.00E-13 2.09E-14 4.00E-12 1.00E-12 6/30/1982 4.69E-15 5.00E-12 1.25E-12 3.46E-15 8.00E-14 2.00E-14 2.38E-15 2.00E-12 S.OOE-13 2.14E-14 4.00E-12 1.00E-12 9/27/1982 4.45E-15 5.00E-12 1.25E-12 3.29E-15 8.00E-14 2.00E-14 3.23E-15 2.00E-12 5.00E-13 1.99E-14 4.00E-12 1.00E-12 1/3/1983 4.39E-15 5.00E-12 1.25E-12 5.91E-16 8.00E-14 2.00E-14 9.14E-16 2.00E-12 5.00E-13 4.87E-14 4.00E-12 1.00E-12 4/4/1983 7.51E-16 5.00E-12 1.25E-12 2.13E-16 8.00E-14 2.00E-14 3.20E-16 2.00E-12 5.00E-13 1.88E-14 4.00E-12 1.00E-12 6/30/1983 2.68E-16 5.00E-12 1.25E-12 6.92E-16 8.00E-14 2.00E-14 7.92E-16 2.00E-12 5.00E-13 2.00E-14 4.00E-12 1.00E-12 10/3/1983 5.00E-12 1.25E-12 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 5.00E-13 4.00E-12 1.00E-12 1/3/1984 2.87E-15 5.00E-12 1.25E-12 1.14E-16 8.00E-14 2.00E-14 1.79E-16 2.00E-12 5.00E-13 1.06E-14 4.00E-12 1.00E-12 4/2/1984 1.59E-15 5.00E-12 1.25E-12 3.40E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 5.00E-13 3.34E-14 4.00E-12 1.00E-12 7/2/1984 3.10E-15 5.00E-12 1.25E-12 1.00E-15 8.00E-14 2.00E-14 2.09E-15 2.00E-12 5.00E-13 1.88E-14 4.00E-12 1.00E-12 10/1/1984 6.42E-16 5.00E-12 1.25E-12 1.39E-16 8.00E-14 2.00E-14 1.94E-16 2.00E-12 5.00E-13 1.85E-14 4.00E-12 1.00E-12 1/2/1985 5.06E-16 5.00E-12 1.25E-12 4.56E-16 8.00E-14 2.00E-14 3.49E-16 2.00E-12 5.00E-13 3.03E-14 4.00E-12 1.00E-12 4/1/1985 O.OOE+OO 5.00E-12 1.25E-12 1.23E-15 8.00E-14 2.00E-14 4.88E-16 2.00E-12 5.00E-13 8.06E-15 4.00E-12 1.00E-12 7/1/1985 7.17E-16 5.00E-12 1.25E-12 8.00E-14 2.00E-14 LOSE-IS 2.00E-12 5.00E-13 2.15E-14 4.00E-12 1.00E-12 9/30/1985 6.13E-16 5.00E-12 1.25E-12 1.18E-16 8.00E-14 2.00E-14 3.7lE-16 2.00E-12 5.00E-13 3.64E-15 4.00E-12 1.00E-12 1/2/1986 3.42E-15 5.00E-12 1.25E-12 4.74E-16 8.00E-14 2.00E-14 2.00E-12 5.00E-13 4.00E-12 1.00E-12 4/1/1986 3.98E-15 5.00E-12 1.25E-12 9.74E-16 8.00E-14 2.00E-14 1.50E-15 2.00E-12 5.00E-13 1.41E-14 4.00E-12 1.00E-12 6/30/1986 5.5lE-17 5.00E-12 1.25E-12 3.52E-16 8.00E-14 2.00E-14 1.37E-15 2.00E-12 5.00E-13 1.23E-14 4.00E-12 1.00E-12 10/27/1986 1.99E-15 5.00E-12 1.25E-12 3.06E-16 8.00E-14 2.00E-14 1.25E-15 2.00E-12 5.00E-13 1.08E-14 4.00E-12 1.00E-12 12/15/1986 1.67E-15 5.00E-12 1.25E-12 1.16E-16 8.00E-14 2.00E-14 5.98E-16 2.00E-12 5.00E-13 1.37E-14 4.00E-12 1.00E-12 3/16/1987 2.33E-15 5.00E-12 1.25E-12 4.30E-16 8.00E-14 2.00E-14 1.92E-16 2.00E-12 5.00E-13 5.59E-14 4.00E-12 1.00E-12 5/11/1987 2.36E-15 5.00E-12 1.25E-12 7.69E-16 8.00E-14 2.00E-14 8.76E-16 2.00E-12 5.00E-13 1.45E-14 4.00E-12 1.00E-12 9/9/1987 2.27E-15 5.00E-12 1.25E-12 2.44E-15 8.00E-14 2.00E-14 8.51E-16 2.00E-12 5.00E-13 3.14E-14 4.00E-12 1.00E-12 11/2/1987 2.75E-15 5.00E-12 1.25E-12 2.46E-15 8.00E-14 2.00E-14 1.34E-15 2.00E-12 5.00E-13 2.79E-14 4.00E-12 1.00E-12 2/16/1988 1.07E-15 5.00E-12 1.25E-12 1.47E-16 8.00E-14 2.00E-14 4.44E-16 2.00E-12 5.00E-13 4.0lE-14 4.00E-12 1.00E-12 5/18/1988 1.98E-15 5.00E-12 1.25E-12 1.25E-15 8.00E-14 2.00E-14 6.40E-16 2.00E-12 5.00E-13 1.07E-14 4.00E-12 1.00E-12 8/15/1988 2.06E-15 5.00E-12 1.25E-12 3.41E-15 8.00E-14 2.00E-14 5.08E-16 2.00E-12 5.00E-13 1.62E-14 4.00E-12 1.00E-12 11/14/1988 3.94E-15 5.00E-12 1.25E-12 2.12E-15 8.00E-14 2.00E-14 1.01E-15 2.00E-12 5.00E-13 2.47E-14 4.00E-12 1.00E-12 2/13/1989 1.99E-15 5.00E-12 1.25E-12 5.73E-16 8.00E-14 2.00E-14 5.99E-16 2.00E-12 5.00E-13 3.23E-14 4.00E-12 1.00E-12 5/15/1989 1.70E-15 5.00E-12 1.25E-12 6.32E-16 8.00E-14 2.00E-14 5.86E-16 2.00E-12 5.00E-13 6.16E-15 4.00E-12 1.00E-12 8/14/1989 2.3lE-15 5.00E-12 1.25E-12 2.31E-16 8.00E-14 2.00E-14 1.77E-16 2.00E-12 5.00E-13 7.65E-15 4.00E-12 1.00E-12 11/13/1989 4.72E-15 5.00E-12 1.25E-12 1.71E-15 8.00E-14 2.00E-14 1.52E-15 2.00E-12 5.00E-13 1.89E-14 4.00E-12 1.00E-12 2/12/1990 3.44E-16 5.00E-12 1.25E-12 8.39E-16 8.00E-14 2.00E-14 8.31E-16 2.00E-12 5.00E-13 2.57E-14 4.00E-12 1.00E-12 5/14/1990 3.03E-15 5.00E-12 1.25E-12 1.47E-15 8.00E-14 2.00E-14 1.04E-15 2.00E-12 5.00E-13 1.79E-14 4.00E-12 1.00E-12 8/13/1990 1.64E-15 5.00E-12 1.25E-12 1.49E-15 8.00E-14 2.00E-14 3.34E-16 2.00E-12 5.00E-13 8.27E-15 4.00E-12 1.00E-12 11/12/1990 1.48E-15 5.00E-12 1.25E-12 7.50E-16 8.00E-14 2.00E-14 5.80E-16 2.00E-12 5.00E-13 2.16E-14 4.00E-12 1.00E-12 2/11/1991 1.90E-16 5.00E-12 1.25E-12 3.48E-17 8.00E-14 2.00E-14 7.9lE-17 2.00E-12 5.00E-13 3.79E-14 4.00E-12 1.00E-12 5/13/1991 3.42E-16 5.00E-12 1.25E-12 1.34E-15 8.00E-14 2.00E-14 7.39E-16 2.00E-12 5.00E-13 1.46E-14 4.00E-12 1.00E-12 8/12/1991 2.77E-16 5.00E-12 1.25E-12 4.17E-17 8.001'-14 2.00E-14 1.45E-16 2.00E-12 5.00E-13 1.80E-14 4.00E-12 1.00E-12 11/11/1991 6.65E-17 5.00E-12 1.25E-12 9.13E-17 8.00E-14 2.00E-14 2.77E-17 2.00E-12 5.00E-13 1.06E-14 4.00E-12 1.00E-12 2/10/1992 1.94E-16 5.00E-12 1.25E-12 4.28E-17 8.00E-14 2.00E-14 4.08E-17 2.00E-12 5.00E-13 3.51E-14 4.00E-12 1.00E-12 5/11/1992 2.54E-16 5.00E-12 1.25E-12 6.49E-16 8.00E-14 2.00E-14 6.86E-17 2.00E-12 5.00E-13 1.38E-14 4.00E-12 1.00E-12 8/10/1992 1.73E-16 5.00E-12 1.25E-12 1.55E-16 8.00E-14 2.00E-14 1.20E-16 2.00E-12 5.00E-13 1.53E-14 4.00E-12 1.00E-12 11/9/1992 1.56E-16 5.00E-12 1.25E-12 3.19E-17 8.00E-14 2.00E-14 4.90E-18 2.00E-12 5.00E-13 1.86E-14 4.00E-12 1.00E-12 2/9/1993 2.10E-16 5.00E-12 1.25E-12 8.00E-14 2.00E-14 3.89E-17 2.00E-12 5.00E-13 2.52E-14 4.00E-12 1.00E-12 5/10/1993 1.00E-16 5.00E-12 1.25E-12 4.11E-17 8.00E-14 2.00E-14 6.43E-17 2.00E-12 5.00E-13 1.26E-14 4.00E-12 1.00E-12 8/10/1993 2.30E-16 5.00E-12 1.25E-12 6.00E-17 8.00E-14 2.00E-14 6.43E-17 2.00E-12 5.00E-13 1.60E-14 4.00E-12 1.00E-12 11/8/1993 5.00E-12 1.25E-12 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 5.00E-13 1.57E-14 4.00E-12 1.00E-12 2/7/1994 1.82E-16 5.00E-12 1.25E-12 5.00E-18 8.00E-14 2.00E-14 4.30E-17 2.00E-12 5.00E-13 2.59E-14 4.00E-12 1.00E-12 5/9/1994 3.60E-16 5.00E-12 1.25E-12 2.70E-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 5.00E-13 1.60E-14 4.00E-12 1.00E-12 8/9/1994 4.04E-16 5.00E-12 1.25E-12 2.70E-16 8.00E-14 2.00E-14 2.94E-16 2.00E-12 5.00E-13 2.00E-15 4.00E-12 1.00E-12 11/7/1994 9.18E-17 5.00E-12 1.25E-12 3.60E-16 8.00E-14 2.00E-14 2.9lE-16 2.00E-12 5.00E-13 2.00E-15 4.00E-12 1.00E-12 2/7/1995 1.77E-16 9.00E-14 2.25E-14 9.70E-17 2.00E-14 5.00E-15 9.70E-17 9.00E-13 2.25E-13 8.60E-15 6.00E-13 1.50E-13 5/9/1995 9.40E-17 9.00E-14 2.25E-14 5.36E-16 2.00E-14 5.00E-15 1.60E-15 9.00E-13 2.25E-13 3.84E-15 6.00E-13 1.50E-13 8/9/1995 2.70E-16 9.00E-14 2.25E-14 1.60E-16 2.00E-14 5.00E-15 2.76E-16 9.00E-13 2.25E-13 3.76E-15 6.00E-13 1.50E-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-lU Effluent Concentration Limit = 2E-14 uCi/ml BHV-1T Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = 6E-13 uCi/ml BHV-1PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 11/11/1995 4.80E-1s 9.00E-14 2.2sE-14 6.41E-16 2.00E-14 s.00E-1s 8.93E-16 9.00E-13 2.2sE-13 s.20E-1s 6.00E-13 1.s0E-13 2/5/1996 s.34E-1s 9.00E-14 2.2sE-14 2.30E-1s 2.00E-14 s.00E-1s l.30E-1s 9.00E-13 2.2sE-13 4.20E-1s 6.00E-13 1.s0E-13 5/6/1996 s.11E-16 9.00E-14 2.2sE-14 3.06E-16 2.00E-14 s.00E-1s 1.40E-16 9.00E-13 2.2sE-13 7.03E-1s 6.00E-13 1.s0E-13 8/5/1996 s.99E-16 9.00E-14 2.2sE-14 1.ssE-1s 2.00E-14 s.00E-1s 2.03E-16 9.00E-13 2.2sE-13 s.94E-1s 6.00E-13 1.s0E-13 11/6/1996 3.38E-16 9.00E-14 2.2sE-14 s.4sE-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.22E-14 6.00E-13 1.s0E-13 2/6/1997 1.00E-16 9.00E-14 2.2sE-14 1.2sE-16 2.00E-14 s.00E-1s 1.28E-16 9.00E-13 2.2sE-13 s.68E-1s 6.00E-13 1.s0E-13 5/5/1997 1.09E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 4.39E-1s 6.00E-13 1.s0E-13 8/11/1997 2.88E-16 9.00E-14 2.2sE-14 3.83E-16 2.00E-14 s.00E-1s 1.82E-16 9.00E-13 2.2sE-13 s.29E-1s 6.00E-13 1.s0E-13 1/5/1998 3.24E-16 9.00E-14 2.2sE-14 3.47E-16 2.00E-14 s.00E-1s 1.19E-16 9.00E-13 2.2sE-13 4.73E-1s 6.00E-13 1.s0E-13 4/28/1998 4.7sE-16 9.00E-14 2.2sE-14 6.73E-16 2.00E-14 s.00E-1s s.69E-16 9.00E-13 2.2sE-13 s.94E-1s 6.00E-13 1.s0E-13 7/31/1998 8.84E-16 9.00E-14 2.2sE-14 1.93E-1s 2.00E-14 s.00E-1s 1.43E-1s 9.00E-13 2.2sE-13 s.22E-1s 6.00E-13 1.s0E-13 9/28/1998 2.81E-16 9.00E-14 2.2sE-14 2.89E-16 2.00E-14 s.00E-1s 1.80E-16 9.00E-13 2.2sE-13 4.64E-1s 6.00E-13 1.s0E-13 12/28/1998 8.08E-16 9.00E-14 2.2sE-14 4.93E-16 2.00E-14 s.00E-1s s.01E-16 9.00E-13 2.2sE-13 1.06E-14 6.00E-13 1.s0E-13 3/29/1999 2.06E-16 9.00E-14 2.2sE-14 2.06E-16 2.00E-14 s.00E-1s 1.42E-16 9.00E-13 2.2sE-13 6.69E-1s 6.00E-13 1.s0E-13 7/3/1999 s.31E-16 9.00E-14 2.2sE-14 2.47E-16 2.00E-14 s.00E-1s 2.23E-16 9.00E-13 2.2sE-13 6.44E-1s 6.00E-13 1.s0E-13 9/27/1999 8.98E-16 9.00E-14 2.2sE-14 3.90E-16 2.00E-14 s.00E-1s 2.96E-16 9.00E-13 2.2sE-13 7.29E-1s 6.00E-13 1.s0E-13 • 12/28/1999 1.48E-1s 9.00E-14 2.2sE-14 6.00E-16 2.00E-14 s.00E-1s s.s7E-16 9.00E-13 2.2sE-13 6.19E-1s 6.00E-13 1.s0E-13 3/27/2000 1.00E-16 9.00E-14 2.2sE-14 1.06E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 6.23E-1s 6.00E-13 1.s0E-13 6/26/2000 3.47E-16 9.00E-14 2.2sE-14 3.46E-16 2.00E-14 s.00E-1s 3.62E-16 9.00E-13 2.2sE-13 4.s0E-1s 6.00E-13 1.s0E-13 9/26/2000 2.s1E-16 9.00E-14 2.2sE-14 1.78E-16 2.00E-14 s.00E-1s 3.2sE-16 9.00E-13 2.2sE-13 8.ssE-1s 6.00E-13 1.s0E-13 12/26/2000 1.00E-16 9.00E-14 2.2sE-14 1.42E-16 2.00E-14 s.00E-1s l.31E-16 9.00E-13 2.2sE-13 7.77E-1s 6.00E-13 1.s0E-13 3/26/2001 3.10E-16 9.00E-14 2.2sE-14 1.00E-1s 2.00E-14 s.00E-1s 1.00E-1s 9.00E-13 2.2sE-13 7.19E-1s 6.00E-13 1.s0E-13 7/29/2001 1.s2E-16 9.00E-14 2.2sE-14 1.44E-16 2.00E-14 s.00E-1s 1.77E-16 9.00E-13 2.2sE-13 7.21E-1s 6.00E-13 1.s0E-13 9/24/2001 1.03E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 8.09E-1s 6.00E-13 1.s0E-13 12/31/2001 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 l.39E-1s 6.00E-13 1.s0E-13 4/1/2002 2.0sE-16 9.00E-14 2.2sE-14 2.44E-16 2.00E-14 s.00E-1s 2.29E-16 9.00E-13 2.2sE-13 8.1sE-1s 6.00E-13 1.s0E-13 7/1/2002 3.ssE-16 9.00E-14 2.2sE-14 4.8sE-16 2.00E-14 s.00E-1s 1.06E-16 9.00E-13 2.2sE-13 7.6sE-1s 6.00E-13 1.s0E-13 9/30/2002 1.17E-16 9.00E-14 2.2sE-14 1.61E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 3.68E-1s 6.00E-13 1.s0E-13 12/30/2002 1.00E-16 9.00E-14 2.2sE-14 1.03E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 9.46E-1s 6.00E-13 1.s0E-13 3/31/2003 1.20E-16 9.00E-14 2.2sE-14 1.12E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 4.68E-1s 6.00E-13 1.50E-13 6/30/2003 2.18E-16 9.00E-14 2.2sE-14 3.40E-16 2.00E-14 s.00E-1s 1.67E-16 9.00E-13 2.2sE-13 s.96E-1s 6.00E-13 1.s0E-13 9/29/2003 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 7.28E-1s 6.00E-13 1.s0E-13 12/29/2003 1.00E-16 9.00E-14 2.2sE-14 2.s4E-16 2.00E-14 s.00E-1s 3.3sE-16 9.00E-13 2.2sE-13 6.2sE-1s 6.00E-13 1.s0E-13 3/29/2004 1.00E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.S4E-14 6.00E-13 1.S0E-13 6/27/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 3.04E-1S 6.00E-13 1.S0E-13 9/27/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.0SE-14 6.00E-13 1.S0E-13 12/27/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 s .00E-1S 1.00E-16 9.00E-13 2.2sE-13 1.S9E-14 6.00E-13 1.s0E-13 3/28/2005 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 s .00E-1S 1.00E-16 9.00E-13 2.2sE-13 7.42E-1s 6.00E-13 1.S0E-13 6/29/2005 1.00E-16 9.00E-14 2.2sE-14 1.30E-16 2.00E-14 s .00E-1S 1.20E-16 9.00E-13 2.2SE-13 7.94E-1S 6.00E-13 1.S0E-13 9/26/2005 1.00E-16 9.00E-14 2.2SE-14 2.S6E-16 2.00E-14 S.00E-1S 2.42E-16 9.00E-13 2.2SE-13 1.22E-14 6.00E-13 1.S0E-13 1/3/2006 2.13E-16 9.00E-14 2.2SE-14 1.04E-16 2.00E-14 S.00E-1s 1.00E-16 9.00E-13 2.2SE-13 3.73E-14 6.00E-13 1.s0E-13 4/3/2006 1.62E-16 9.00E-14 2.2SE-14 1.86E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 8.36E-1S 6.00E-13 1.S0E-13 7/3/2006 1.86E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 9.77E-1S 6.00E-13 1.S0E-13 10/2/2006 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2sE-13 l.30E-14 6.00E-13 1.s0E-13 1/1/2007 1.00E-16 9.00E-14 2.2SE-14 1.47E-16 2.00E-14 s.00E-1S 1.00E-16 9.00E-13 2.2sE-13 1.17E-14 6.00E-13 1.s0E-13 4/2/2007 2.23E-16 9.00E-14 2.2SE-14 1.63E-16 2.00E-14 s.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.6SE-14 6.00E-13 1.S0E-13 7/2/2007 3.3sE-16 9.00E-14 2.2SE-14 1.34E-16 2.00E-14 S.00E-1S l.36E-16 9.00E-13 2.2SE-13 1.78E-14 6.00E-13 1.S0E-13 9/30/2007 1.lSE-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 7.68E-1S 6.00E-13 1.S0E-13 12/31/2007 1.00E-16 9.00E-14 2.2SE-14 1.93E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.31E-14 6.00E-13 1.50E-13 3/31/2008 1.14E-16 9.00E-14 2.2SE-14 1.13E-16 2.00E-14 s.00E-1S 1.00E-16 9.00E-13 2.2sE-13 6.44E-1S 6.00E-13 1.S0E-13 6/30/2008 7.09E-16 9.00E-14 2.2SE-14 3.83E-16 2.00E-14 s.00E-1S 2.27E-16 9.00E-13 2.2sE-13 6.S2E-1s 6.00E-13 1.S0E-13 9/30/2008 7.69E-16 9.00E-14 2.2SE-14 2.94E-16 2.00E-14 S.00E-1S 1.90E-16 9.00E-13 2.2SE-13 7.64E-1S 6.00E-13 1.S0E-13 12/31/2008 1.21E-1S 9.00E-14 2.2SE-14 4.76E-16 2.00E-14 S.00E-1S 3.34E-16 9.00E-13 2.2SE-13 1.16E-14 6.00E-13 1.S0E-13 3/15/2009 2.14E-1S 9.00E-14 2.2SE-14 1.02E-1S 2.00E-14 S.00E-1S 1.00E-1S 9.00E-13 2.2sE-13 4.44E-1S 6.00E-13 1.S0E-13 6/15/2009 S.97E-17 9.00E-14 2.2sE-14 2.3SE-16 2.00E-14 s.00E-1S 2.18E-16 9.00E-13 2.2SE-13 S.13E-1S 6.00E-13 1.s0E-13 9/15/2009 9.SSE-16 9.00E-14 2.2SE-14 1.71E-16 2.00E-14 S.00E-1S 9.87E-17 9.00E-13 2.2SE-13 9.47E-1S 6.00E-13 1.S0E-13 12/15/2009 1.24E-1S 9.00E-14 2.2SE-14 9.2SE-17 2.00E-14 S.00E-1S s.60E-17 9.00E-13 2.2SE-13 S.9sE-1S 6.00E-13 1.S0E-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-1U Effluent Concentration Limit = 2E-14 uCi/ml BHV-1T Effluent Concentration Limit = 9E-13 uCi/ml BHV-1R Effluent Concentration Limit = 6E-13 uCi/ml BHV-1PB ALARA Goal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal = 2.2SE-13 uCi/ml ALARA Goal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 3/31/2010 1.97E-1S 9.00E-14 2.2SE-14 2.1SE-16 2.00E-14 S.00E-1S 3.27E-16 9.00E-13 2.2SE-13 1.00E-14 6.00E-13 l.S0E-13 6/30/2010 l.S8E-1S 9.00E-14 2.2SE-14 4.71E-16 2.00E-14 S.00E-1S 7.70E-16 9.00E-13 2.2SE-13 4.07E-1S 6.00E-13 l.S0E-13 9/30/2010 8.42E-16 9.00E-14 2.2SE-14 2.80E-16 2.00E-14 S.00E-1S l.31E-16 9.00E-13 2.2SE-13 6.80E-1S 6.00E-13 l.S0E-13 12/31/2010 1.27E-1S 9.00E-14 2.2SE-14 2.32E-16 2.00E-14 S.00E-1S 2.30E-16 9.00E-13 2.2SE-13 1.27E-14 6.00E-13 l.S0E-13 4/4/2011 9.0lE-16 9.00E-14 2.2SE-14 1.90E-16 2.00E-14 S.00E-1S 3.64E-16 9.00E-13 2.2SE-13 1.09E-14 6.00E-13 1.S0E-13 7/4/2011 1.S9E-1S 9.00E-14 2.2SE-14 S.3lE-16 2.00E-14 S.00E-1S 4.99E-16 9.00E-13 2.2SE-13 8.38E-1S 6.00E-13 l.S0E-13 10/3/2011 2.92E-16 9.00E-14 2.2SE-14 1.17E-16 2.00E-14 S.00E-1S 6.76E-17 9.00E-13 2.2SE-13 1.14E-14 6.00E-13 l.S0E-13 1/3/2012 6.73E-16 9.00E-14 2.2SE-14 1.19E-16 2.00E-14 S.00E-1S 8.S8E-17 9.00E-13 2.2SE-13 1.73E-14 6.00E-13 l.S0E-13 4/3/2012 7.87E-16 9.00E-14 2.2SE-14 2.64E-16 2.00E-14 S.00E-1S 3.9SE-16 9.00E-13 2.2SE-13 1.2SE-14 6.00E-13 l.S0E-13 7/2/2012 1.86E-1S 9.00E-14 2.2SE-14 8.33E-16 2.00E-14 S.00E-1S 9.8SE-16 9.00E-13 2.2SE-13 9.SSE-1S 6.00E-13 l.S0E-13 -E :::: (J :::J -tn r:::: o ;:; e ..... r:::: CI) o r:::: o (J CI) "C o :::J r:::: o "C ns 0::: N ~ I W o o C") ~ I W o o .;;t ~ I W o o IIII ~ Iii . l . ""'~I fll ~ !.;. .: ...... ~ i i r~ ~. i ~1 i ~ ~~ i ! lil ~· LO c.o ~ ~ I I W W 0 0 ~ ~ ~ ~ (ale~s 501) ~ ~-das o~-das 60-daS go-das LO-daS go-das go-das Po-das 0 ~ £O-daS N I "'0 co lO-daS Q) .....J ~o-das t OO-daS c.o N N 66-daS I E .~ 96-daS "'0 co 0::: L6-daS t 96-daS 0 96-daS C"') N I P6-daS E :::J ·c 0 Ii £6-das ..c I I l-Ii t l6-daS ~6-das ro L.. 06-daS :::J 10 z 69-daS E :::J gg-daS ·c co L.. => L9-daS t gg-daS gg-daS pg-das £g-daS 19-daS ~g-das I"-00 ~ ~ I I W W 0 0 ~ ~ Effluent Concentration Limit = 2E-14 uCi/ml ALARA Goal = 5E-13 uCilml Pre 1994 MPC Limit = 8E-14uCi/ml BHV-1 Thorium-230 Concentrations (uCi/ml) 1 .00 E -12 F~~~:~=7.~~7.=7.='~~::~=:~:='~~:=~=::~::~:=.:::=~="=.~=::::= .. =.=:=.= .. =::~:::== .. ~=~:=-:=:::;=.::~=.=.:=.:==.:=.=:::::=.=.:-:= .. =:~:==.:=.::==."~=.:::=====:=.:==~=.=::~::=::=.=.~:=.:==:::::=.=.=::~=~:~:=.== :::::~::::~:=.::::=::::::~:::::::=.::::=-:::::::: ............... ::::::~.:::::::~::::::~::::~:::::~ ..... :::::::::::::::::::~::::~:~:~ .... :::::~~::~::~'::::::::~ ..... ::::~::::~:::~~:~~::~~ ... ""'.::::::::::~~:::::~~::=:::::~ :::::1 1.00E-13 I .. .. . ....... "1 ..... _ .... _ ...................... _ .... c_ ... _ .. _ .......... _ .. _._ ..... _ .......... _ ..... _ ..... _ ...... _ .................................................................... _.............. . ... j::=:::==::::~... . ............... :.:.:::::::::==::::....... .................................................... . ...................... _.......... ::::::::::::::=::::::=:::=::::::=::=:=:::::::::=:::::::=::::::::::=:=::::::::::::::. , ~----------------~,~----------------------~ , 1.00E-14 g~~~~~~~~~~~~~~~E~~~~~~~~~~~~~~~~~~~~ ... . ~ ..... _ ....... _ .. _ ............ _ .. _ ............ _ .. ~ .00 E -15 ...... ................. . C> o .....J -- --.. -:::=~===== .. ====~=:::= .. ===~============~=.=.~=.~=~=.~=.~~~=.~=.~==.=.~=.~=.~=.~=.:=.=.:=.==~:~~~~~~~~~~~~~~~~~~:~~~~~:~== 1.00E-16 .................. . ............................................................ - . ........ __ ...........•. _ ..... . 1.00E-17 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-18 T""" N M -:;t l!) CD I'--00 0> 0 T""" N M -:;t l!) CD I'--00 0> 0 T""" N M -:;t l!) CD I'--00 0> 0 00 00 00 00 00 00 00 00 00 0> 0> 0> 0> 0> 0> 0> 0> 0> 0> 0 0 0 0 0 0 0 0 0 0 T""" T""" I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) en en en en en en en en en en en en en en en en en en en en en en en en en en en en en en en 1.00E-11 Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCilml Pre 1994 ALARA Goal = 5E-13 uCi/ml BHV-1 Radium-226 Concentrations (uCi/ml) 1.ooE-121 ------------------------------~ I --------,-----------------------_._------------------------------------------------_._----_._----------_._--._-----_._ ..... _---_ ... __ .. _ ... __ .. _---_ ... __ ._-_ .. _---_._-_._-_ .. __ .. _-_._-_ ... __ .. __ ._-_ ... _--_ ....... _ ... -_ ............ '._ ....... -............ -.--.-.-.. -.-_ ... _. _._._--._-_._-_._--_._--_._-_._-----_._-_ .... _--_._-_ ..... _-----_ ... __ ..... ---........................ _ .... __ ....... -._ ....... _ .. _--... _._-_._-_ ... __ ... _--_ ... _---_ ........... _-_._--_._ ............ . \ \ 1.00E-13 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ ~. 00 E -14 ~~=====~ ____ --=-~-=-=-=-:.::-.::.:--=-.::.::::::-=--=-.=:.=:~~-.::..-.::.::::::.::..--=--=--=-.::.:-.::::.::..-=_=-=-.::_______ _ ____ ...::::::::::~-.::::.::::.::~-.::::::::::::::.:::::::::::: _________________ . ____ . _______ _ ........ _ ... _ ... _. __ . __ . __ . __ ... _-... :::. .. _ .... __ .-:::::::.:::::::::::::::::::::::::::::::: ......•.... : .... : .. : .. -.... . ................................. _ ..... -............... -...... _ .. () CI) ~.OOE-15 .-:~~~~~~~~~-=-~~==-=._ 1. OOE-16 --.... -""" .... __ ,,_c.c=_.cc... _. _______ ~.=.=====--_-- -------------------------- --- ----- 1.00E-17 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-18 T""" N ('f) ""'" LO co "-00 0> 0 T""" N ('f) ""'" LO co "-00 0> 0 T""" N ('f) ""'" LO co "-00 0> 0 00 00 00 00 00 00 00 00 00 0> 0> 0> 0> 0> 0> 0> 0> 0> 0> 0 0 0 0 0 0 0 0 0 0 T""" T""" I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CI) CI) CI) CI) CI) CI) CI) CI) CI) CJ) CJ) CI) CJ) CJ) CJ) CI) CI) CI) CI) CI) CJ) CJ) CJ) CJ) CJ) CJ) CI) CI) CI) CI) CI) 1.00E-11 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1 E-12 uCi/ml BHV-1 Lead-210 Concentrations (uCi/ml) , 1.00E-12 ~~~~='~~~-=-~~=!:====:.-~======~-j I 1.00E-13 E~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ Q) co b.1.00E-14 0') o d- l 1.00E-15 E~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-16 E~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-17 ~ C\I ('I") .q-L() <0 r--.. co 0) 0 ~ C\I ('I") .q-L() <0 r--.. co 0) 0 ~ C\I ('I") .q-L() <0 r--.. co 0) 0 co co co co co co co co co 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0 0 0 0 0 0 0 0 0 0 ~ ~ I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) en en en en en en en en en en en en en en en en en en en en en en en en en en en en en en en TAB 2 BHV-2 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-2U Effluent Concentration Limit = 2E-14 uCi/ml BHV-2T Effluent Concentration Limit = 9E-13 uCi/ml BHV-2R Effluent Concentration Limit = 6E-13 uCi/ml BHV-2PB I ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml I Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 1.39E-1S S.00E-12 l.2SE-12 3.69E-16 8.00E-14 2.00E-14 S.92E-16 2.00E-12 S.OOE-13 l.67E-14 4.00E-12 l.OOE-12 12/14/1981 4.62E-16 S.00E-12 1.2SE-12 8.03E-16 8.00E-14 2.00E-14 3.62E-16 2.00E-12 S.OOE-13 1.33E-14 4.00E-12 l.OOE-12 3/29/1982 7.07E-16 S.00E-12 l.2SE-12 l.lOE-1S 8.00E-14 2.00E-14 7.27E-16 2.00E-12 S.OOE-13 1.S2E-14 4.00E-12 l.OOE-12 6/30/1982 8.84E-16 S.OOE-12 l.2SE-12 7.73E-16 8.00E-14 2.00E-14 4.78E-16 2.00E-12 S.OOE-13 l.98E-14 4.00E-12 l.OOE-12 9/27/1982 l.23E-1S S.00E-12 l.2SE-12 3.60E-16 8.00E-14 2.00E-14 8.73E-16 2.00E-12 S.OOE-13 2.3SE-14 4.00E-12 l.OOE-12 1/3/1983 2.64E-1S S.00E-12 l.2SE-12 2.SSE-16 8.00E-14 2.00E-14 l.98E-16 2.00E-12 S.OOE-13 2.8SE-14 4.00E-12 l.OOE-12 4/4/1983 2.14E-16 S.00E-12 l.2SE-12 l.02E-16 8.00E-14 2.00E-14 l.S7E-16 2.00E-12 S.OOE-13 2.48E-14 4.00E-12 1.00E-12 6/30/1983 2.8SE-16 S.00E-12 1.2SE-12 2.06E-16 8.00E-14 2.00E-14 2.24E-16 2.00E-12 S.OOE-13 l.79E-14 4.00E-12 l.OOE-12 10/3/1983 2.70E-16 S.00E-12 l.2SE-12 3.36E-16 8.00E-14 2.00E-14 4.37E-16 2.00E-12 S.OOE-13 l.78E-14 4.00E-12 l.OOE-12 1/3/1984 2.78E-1S S.OOE-12 l.2SE-12 l.20E-16 8.00E-14 2.00E-14 6.64E-17 2.00E-12 S.OOE-13 9.14E-1S 4.00E-12 l.OOE-12 4/2/1984 4.28E-16 S.00E-12 l.2SE-12 l.7SE-16 8.00E-14 2.00E-14 4.S7E-17 2.00E-12 S.OOE-13 3.SSE-14 4.00E-12 l.OOE-12 7/2/1984 2.78E-1S S.00E-12 l.2SE-12 8.12E-16 8.00E-14 2.00E-14 l.98E-16 2.00E-12 S.OOE-13 l.68E-14 4.00E-12 l.OOE-12 10/1/1984 2.69E-16 S.00E-12 1.2SE-12 2.66E-17 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 S.OOE-13 l.77E-14 4.00E-12 1.00E-12 1/2/1985 2.lSE-16 S.00E-12 1.2SE-12 7.SSE-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 S.OOE-13 3.19E-14 4.00E-12 l.OOE-12 4/1/1985 l.00E-16 S.00E-12 l.2SE-12 l.67E-16 8.00E-14 2.00E-14 6.7SE-17 2.00E-12 S.OOE-13 7.S6E-1S 4.00E-12 l.OOE-12 7/1/1985 3.70E-17 S.00E-12 l.2SE-12 9.00E-16 8.00E-14 2.00E-14 4.90E-17 2.00E-12 S.OOE-13 1.3lE-14 4.00E-12 l.OOE-12 9/30/1985 9.32E-17 S.00E-12 l.2SE-12 2.18E-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 S.OOE-13 3.64E-1S 4.00E-12 l.OOE-12 1/2/1986 l.00E-16 S.00E-12 1.2SE-12 2.16E-16 8.00E-14 2.00E-14 2.lSE-17 2.00E-12 S.OOE-13 3.04E-16 4.00E-12 l.00E-12 4/1/1986 l.31E-1S S.OOE-12 l.2SE-12 l.SOE-16 8.00E-14 2.00E-14 3.71E-16 2.00E-12 S.OOE-13 2.90E-1S 4.00E-12 l.OOE-12 6/30/1986 2.23E-16 S.00E-12 l.2SE-12 1.32E-16 8.00E-14 2.00E-14 7.09E-17 2.00E-12 S.OOE-13 2.S3E-14 4.00E-12 l.00E-12 10/27/1986 6.4lE-16 S.00E-12 l.2SE-12 l.74E-16 8.00E-14 2.00E-14 3.67E-16 2.00E-12 S.OOE-13 l.04E-14 4.00E-12 l.OOE-12 12/15/1986 3.S6E-16 S.00E-12 l.2SE-12 l.00E-16 8.00E-14 2.00E-14 1.0SE-16 2.00E-12 S.OOE-13 7.81E-1S 4.00E-12 l.OOE-12 3/16/1987 S.31E-16 S.00E-12 1.2SE-12 1.30E-16 8.00E-14 2.00E-14 7.74E-17 2.00E-12 S.OOE-13 3.80E-14 4.00E-12 l.OOE-12 5/11/1987 4.06E-16 S.00E-12 l.2SE-12 6.63E-17 8.00E-14 2.00E-14 1.34E-16 2.00E-12 S.OOE-13 1.10E-14 4.00E-12 l.OOE-12 9/9/1987 2.74E-16 S.00E-12 l.2SE-12 2.38E-16 8.00E-14 2.00E-14 l.38E-16 2.00E-12 S.OOE-13 l.04E-14 4.00E-12 l.00E-12 11/2/1987 3.73E-16 S.00E-12 l.2SE-12 3.11E-16 8.00E-14 2.00E-14 l.83E-16 2.00E-12 S.OOE-13 1.17E-14 4.00E-12 l.OOE-12 2/16/1988 2.78E-1S S.00E-12 l.2SE-12 2.31E-17 8.00E-14 2.00E-14 l.20E-16 2.00E-12 S.OOE-13 3.5SE-14 4.00E-12 l.OOE-12 5/18/1988 4.63E-16 S.00E-12 l.2SE-12 1.49E-16 8.00E-14 2.00E-14 2.30E-16 2.00E-12 S.OOE-13 1.18E-14 4.00E-12 l.OOE-12 8/15/1988 8.06E-16 S.00E-12 l.2SE-12 8.69E-16 8.00E-14 2.00E-14 l.80E-16 2.00E-12 S.OOE-13 l.42E-14 4.00E-12 l.OOE-12 11/14/1988 4.34E-16 S.00E-12 l.2SE-12 6.76E-16 8.00E-14 2.00E-14 l.S7E-16 2.00E-12 S.OOE-13 2.2SE-14 4.00E-12 l.OOE-12 2/13/1989 S.80E-16 S.00E-12 l.2SE-12 2.8SE-16 8.00E-14 2.00E-14 l.SSE-16 2.00E-12 S.OOE-13 2.80E-14 4.00E-12 l.OOE-12 5/15/1989 S.06E-16 S.00E-12 l.2SE-12 2.28E-16 8.00E-14 2.00E-14 1.63E-16 2.00E-12 S.OOE-13 6.0SE-1S 4.00E-12 1.00E-12 8/14/1989 4.7lE-16 S.00E-12 l.2SE-12 9.60E-16 8.00E-14 2.00E-14 l.26E-1S 2.00E-12 S.OOE-13 6.6SE-1S 4.00E-12 l.00E-12 11/13/1989 1.14E-1S S.00E-12 l.2SE-12 4.08E-16 8.00E-14 2.00E-14 4.18E-16 2.00E-12 S.OOE-13 l.S9E-14 4.00E-12 l.00E-12 2/12/1990 l.09E-1S S.00E-12 l.2SE-12 3.2SE-16 8.00E-14 2.00E-14 3.74E-16 2.00E-12 S.OOE-13 1.98E-14 4.00E-12 l.00E-12 5/14/1990 9.32E-16 S.00E-12 l.2SE-12 S.27E-16 8.00E-14 2.00E-14 3.97E-16 2.00E-12 S.OOE-13 l.69E-14 4.00E-12 l.00E-12 8/13/1990 l.66E-16 S.00E-12 l.2SE-12 S.49E-16 8.00E-14 2.00E-14 4.7SE-17 2.00E-12 S.OOE-13 l.27E-1S 4.00E-12 l.OOE-12 11/12/1990 6.0SE-16 S.00E-12 l.2SE-12 2.64E-16 8.00E-14 2.00E-14 l.93E-16 2.00E-12 S.OOE-13 2.2SE-14 4.00E-12 l.OOE-12 2/11/1991 8.72E-17 S.00E-12 l.2SE-12 7.00E-18 8.00E-14 2.00E-14 3.33E-17 2.00E-12 S.OOE-13 3.49E-14 4.00E-12 1.00E-12 5/13/1991 l.16E-16 S.00E-12 l.2SE-12 3.86E-16 8.00E-14 2.00E-14 2.80E-16 2.00E-12 S.OOE-13 l.50E-14 4.00E-12 l.OOE-12 8/12/1991 9.02E-17 S.00E-12 l.2SE-12 8.82E-17 8.00E-14 2.00E-14 7.6SE-17 2.00E-12 S.OOE-13 l.S8E-14 4.00E-12 l.OOE-12 11/11/1991 4.81E-17 S.00E-12 l.2SE-12 3.82E-17 8.00E-14 2.00E-14 2.S4E-17 2.00E-12 S.OOE-13 l.4SE-14 4.00E-12 l.OOE-12 2/10/1992 l.S4E-16 S.00E-12 l.2SE-12 6.82E-17 8.00E-14 2.00E-14 l.40E-17 2.00E-12 S.OOE-13 3.4lE-14 4.00E-12 l.00E-12 5/11/1992 2.38E-16 S.00E-12 l.2SE-12 7.63E-17 8.00E-14 2.00E-14 3.07E-17 2.00E-12 S.OOE-13 l.27E-14 4.00E-12 l.OOE-12 8/10/1992 1.01E-16 S.00E-12 1.2SE-12 7.07E-17 8.00E-14 2.00E-14 2.80E-17 2.00E-12 S.OOE-13 l.41E-14 4.00E-12 l.OOE-12 11/9/1992 S.20E-17 S.00E-12 1.2SE-12 3.6SE-17 8.00E-14 2.00E-14 l.78E-17 2.00E-12 S.OOE-13 l.71E-14 4.00E-12 l.OOE-12 2/9/1993 2.39E-16 S.00E-12 l.2SE-12 2.97E-17 8.00E-14 2.00E-14 6.31E-17 2.00E-12 S.OOE-13 3.41E-14 4.00E-12 l.00E-12 5/10/1993 1.00E-16 S.00E-12 l.2SE-12 7.11E-17 8.00E-14 2.00E-14 3.19E-17 2.00E-12 S.OOE-13 1.34E-14 4.00E-12 l.OOE-12 8/10/1993 1.90E-16 S.00E-12 l.2SE-12 l.00E-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 l.80E-14 4.00E-12 l.OOE-12 11/8/1993 l.00E-16 S.00E-12 l.2SE-12 l.00E-16 8.00E-14 2.00E-14 l.00E-16 2.00E-12 S.OOE-13 l.49E-14 4.00E-12 1.00E-12 2/7/1994 2.23E-16 S.00E-12 l.2SE-12 1.00E-16 8.00E-14 2.00E-14 l.84E-16 2.00E-12 S.OOE-13 2.19E-14 4.00E-12 l.OOE-12 5/9/1994 2.16E-16 S.00E-12 l.2SE-12 7.20E-17 8.00E-14 2.00E-14 9.89E-17 2.00E-12 S.OOE-13 l.37E-14 4.00E-12 l.OOE-12 8/9/1994 9.29E-17 S.00E-12 l.2SE-12 2.96E-16 8.00E-14 2.00E-14 3.04E-16 2.00E-12 S.OOE-13 l.00E-16 4.00E-12 l.00E-12 11/7/1994 9.2lE-17 S.00E-12 l.2SE-12 2.3SE-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 1.00E-16 4.00E-12 1.00E-12 2/7/1995 1.18E-16 9.00E-14 2.2SE-14 9.70E-17 2.00E-14 S.00E-1S 9.70E-17 9.00E-13 2.2SE-13 7.42E-1S 6.00E-13 1.S0E-13 5/9/1995 9.40E-17 9.00E-14 2.2SE-14 1.20E-16 2.00E-14 S.00E-1S 3.SOE-16 9.00E-13 2.2SE-13 3.90E-1S 6.00E-13 1.S0E-13 8/9/1~ __ .~~~O~lL __ . _____ . ___ 9.00E-14 2.2SE-14 9.67E-17 2.00E-14 S.00E-1S 1.3SE-16 9.00E-13 2.2SE-13 2.38E-16 6.00E-13 l.SOE-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-2U Effluent Concentration Limit = 2E-14 uCi/ml BHV-2T Effluent Concentration Limit = 9E-13 uCi/ml BHV-2R Effluent Concentration Limit = 6E-13 uCi/ml BHV-2PB ALARA Goal = 2.25E-14 uCi/ml ALARA Goal = 5E-13 uCi/ml ALARAGoal = 2.25E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 5E-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.25E-12 uCi/ml Pre 1994 ALARA GOAL = 5E-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA 11/11/1995 2.83E-15 9.00E-14 2.25E-14 4.09E-16 2.00E-14 5.00E-15 5.23E-16 9.00E-13 2.25E-13 6.77E-15 6.00E-13 1.50E-13 2/5/1996 1.75E-15 9.00E-14 2.25E-14 8.66E-16 2.00E-14 5.00E-15 4.86E-16 9.00E-13 2.25E-13 3.50E-15 6.00E-13 1.50E-13 5/6/1996 1.40E-16 9.00E-14 2.25E-14 1.15E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.85E-15 6.00E-13 1.50E-13 8/5/1996 1.43E-16 9.00E-14 2.25E-14 2.78E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 5.83E-15 6.00E-13 1.50E-13 11/6/1996 1.45E-16 9.00E-14 2.25E-14 1.57E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.19E-14 6.00E-13 1.50E-13 2/6/1997 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 5.84E-16 6.00E-13 1.50E-13 5/5/1997 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 3.89E-15 6.00E-13 1.50E-13 8/11/1997 1.00E-16 9.00E-14 2.25E-14 1.09E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 5.69E-15 6.00E-13 1.50E-13 1/5/1998 2.55E-16 9.00E-14 2.25E-14 1.07E-16 2.00E-14 5.00E-15 5.00E-17 9.00E-13 2.25E-13 5.l1E-15 6.00E-13 1.50E-13 4/28/1998 1.20E-16 9.00E-14 2.25E-14 1.71E-16 2.00E-14 5.00E-15 1.28E-16 9.00E-13 2.25E-13 6.40E-15 6.00E-13 1.50E-13 7/31/1998 1.47E-16 9.00E-14 2.25E-14 4.24E-16 2.00E-14 5.00E-15 3.39E-16 9.00E-13 2.25E-13 4.80E-15 6.00E-13 1.50E-13 9/28/1998 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 4.26E-15 6.00E-13 1.50E-13 12/28/1998 2.54E-16 9.00E-14 2.25E-14 2.15E-16 2.00E-14 5.00E-15 1.38E-16 9.00E-13 2.25E-13 6.88E-15 6.00E-13 1.50E-13 3/29/1999 1.07E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.61E-15 6.00E-13 1.50E-13 7/3/1999 2.46E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.95E-15 6.00E-13 1.50E-13 9/27/1999 2.81E-16 9.00E-14 2.25E-14 1.41E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.35E-15 6.00E-13 1.50E-13 12/28/1999 5.20E-16 9.00E-14 2.25E-14 2.60E-16 2.00E-14 5.00E-15 2.01E-16 9.00E-13 2.25E-13 7.00E-15 6.00E-13 1.50E-13 3/27/2000 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.12E-15 6.00E-13 1.50E-13 6/26/2000 1.10E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.16E-16 9.00E-13 2.25E-13 5.07E-15 6.00E-13 1.50E-13 9/26/2000 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 5.31E-15 6.00E-13 1.50E-13 12/26/2000 1.26E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 9.45E-15 6.00E-13 1.50E-13 3/26/2001 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.95E-15 6.00E-13 1.50E-13 7/2/2001 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.56E-15 6.00E-13 1.50E-13 9/24/2001 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.16E-15 6.00E-13 1.50E-13 12/31/2001 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 2.20E-15 6.00E-13 1.50E-13 4/1/2002 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 9.95E-15 6.00E-13 1.50E-13 7/1/2002 1.25E-16 9.00E-14 2.25E-14 1.43E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 8.25E-15 6.00E-13 1.50E-13 9/30/2002 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 3.69E-15 6.00E-13 1.50E-13 12/30/2002 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.91E-15 6.00E-13 1.50E-13 3/31/2003 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.16E-15 6.00E-13 1.50E-13 6/30/2003 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 5.27E-15 6.00E-13 1.50E-13 9/29/2003 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.23E-15 6.00E-13 1.50E-13 12/29/2003 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 7.80E-15 6.00E-13 1.50E-13 3/29/2004 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 2.04E-14 6.00E-13 1.50E-13 6/27/2004 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 3.09E-15 6.00E-13 1.50E-13 9/27/2004 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.73E-14 6.00E-13 1.50E-13 12/27/2004 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.30E-14 6.00E-13 1.50E-13 3/28/2005 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 8.88E-15 6.00E-13 1.50E-13 6/29/2005 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 8.85E-15 6.00E-13 1.50E-13 9/26/2005 1.00E-16 9.00E-14 2.25E-14 1.99E-16 2.00E-14 5.00E-15 1.44E-16 9.00E-13 2.25E-13 3.81E-14 6.00E-13 1.50E-13 1/3/2006 1.29E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 4.08E-16 9.00E-13 2.25E-13 6.58E-14 6.00E-13 1.50E-13 4/3/2006 1.02E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.08E-14 6.00E-13 1.50E-13 7/3/2006 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.10E-14 6.00E-13 1.50E-13 10/2/2006 1.30E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.68E-14 6.00E-13 1.50E-13 1/1/2007 1.24E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.38E-14 6.00E-13 1.50E-13 4/2/2007 1.40E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.63E-14 6.00E-13 1.50E-13 7/2/2007 1.04E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.36E-14 6.00E-13 1.50E-13 9/30/2007 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 8.24E-15 6.00E-13 1.50E-13 12/31/2007 1.91E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 1.18E-14 6.00E-13 1.50E-13 3/30/2008 1.00E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 6.49E-15 6.00E-13 1.50E-13 6/30/2008 1.29E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 4.82E-15 6.00E-13 1.50E-13 9/30/2008 2.73E-16 9.00E-14 2.25E-14 1.00E-16 2.00E-14 5.00E-15 1.00E-16 9.00E-13 2.25E-13 8.30E-15 6.00E-13 1.50E-13 12/31/2008 5.71E-16 9.00E-14 2.25E-14 1.61E-16 2.00E-14 5.00E-15 1.25E-16 9.00E-13 2.25E-13 2.04E-14 6.00E-13 1.50E-13 3/15/2009 3.96E-16 9.00E-14 2.25E-14 1.38E-16 2.00E-14 5.00E-15 1.07E-16 9.00E-13 2.25E-13 4.81E-15 6.00E-13 1.50E-13 6/15/2009 1.24E-17 9.00E-14 2.25E-14 4.64E-17 2.00E-14 5.00E-15 5.11E-17 9.00E-13 2.25E-13 4.58E-15 6.00E-13 1.50E-13 9/15/2009 2.43E-16 9.00E-14 2.25E-14 5.28E-17 2.00E-14 5.00E-15 4.84E-17 9.00E-13 2.25E-13 1.19E-14 6.00E-13 1.50E-13 12/15/2009 5.72E-16 9.00E-14 2.25E-14 2.94E-17 2.00E-14 5.00E-15 2.57E-17 9.00E-13 2.25E-13 6:70E-15 6.00E-13 1.50E-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-2U Effluent Concentration Limit = 2E-14 uCi/ml BHV-2T Effluent Concentration Limit = 9E-13 uCi/ml BHV-2R Effluent Concentration Limit = 6E-13 uCi/ml BHV-2PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = l.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 3/31/2010 S.47E-16 9.00E-14 2.2SE-14 l.42E-17 2.00E-14 S.00E-1S 4.66E-17 9.00E-13 2.2SE-13 8.24E-1S 6.00E-13 l.50E-13 6/30/2010 3.S8E-16 9.00E-14 2.2SE-14 6.64E-17 2.00E-14 S.00E-1S 9.90E-17 9.00E-13 2.2SE-13 2.01E-1S 6.00E-13 l.SOE-13 9/30/2010 2.91E-16 9.00E-14 2.2SE-14 4.48E-17 2.00E-14 S.00E-1S S.72E-17 9.00E-13 2.2SE-13 l.08E-1S 6.00E-13 l.SOE-13 12/31/2010 S.73E-16 9.00E-14 2.2SE-14 7.24E-17 2.00E-14 S.00E-1S 6.76E-17 9.00E-13 2.2SE-13 l.3SE-14 6.00E-13 1.S0E-13 4/4/2011 3.79E-16 9.00E-14 2.2SE-14 4.0lE-17 2.00E-14 S.00E-1S 9.11E-17 9.00E-13 2.2SE-13 l.06E-14 6.00E-13 l.SOE-13 7/4/2011 3.07E-16 9.00E-14 2.2SE-14 8.S4E-17 2.00E-14 S.00E-1S 9.21E-17 9.00E-13 2.2SE-13 7.2lE-1S 6.00E-13 l.SOE-13 10/3/2011 1.17E-16 9.00E-14 2.2SE-14 3.04E-17 2.00E-14 S.00E-1S 2.81E-17 9.00E-13 2.2SE-13 l.03E-14 6.00E-13 l.SOE-13 1/3/2012 3.6SE-16 9.00E-14 2.2SE-14 2.72E-17 2.00E-14 S.00E-1S 4.S4E-17 9.00E-13 2.2SE-13 l.S8E-14 6.00E-13 l.SOE-13 4/3/2012 4.22E-16 9.00E-14 2.2SE-14 l.lSE-16 2.00E-14 S.00E-1S 2.77E-16 9.00E-13 2.2SE-13 l.S8E-14 6.00E-13 l.SOE-13 7/2/2012 3.39E-16 9.00E-14 2.2SE-14 1.S6E-16 2.00E-14 S.00E-1S 1.74E-16 9.00E-13 2.2SE-13 8.60E-1S 6.00E-13 l.SOE-13 -E ::: U :J - N T""" I W 0 ~ ('I') T""" I W 0 ~ ~m'i i i i ! ! I ~ II I ...;;:t l!) <0 T""" T""" T""" I I I W W W 0 0 0 ~ ~ ~ T""" T""" (al8os 501) ~ ~-das o~-das 60-daS go-das LO-daS go-das go-das Po-das 0 T""" £O-daS N I "'C co lO-daS Q) ~ ~o-das t OO-daS <0 N N 66-daS I E :J g6-daS ~ co 0::: L6-daS t 96-daS 0 96-daS ('I') N I P6-daS E :J °C 0 £6-daS ..c I- l6-daS t ~6-das ro '- 06-daS :J ro z 6g-daS E o~ gg-daS c co '-::J Lg-daS t gg-daS gg-daS pg-daS £g-daS 19-daS ~g-das I'--co T""" T""" I I W W 0 0 ~ ~ T""" 1.00E-11 Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml BHV-2 Uranium-Natural Concentrations (uCi/ml) 1.00E-12 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-13 1----.. --------------·t I ...... __ ... __ ... __ ... __ ... __ ... __ ....•.•..•........•..•. _ ............. _ ....... _-_ ....... ' ......... _._ .•. -._.'.-"----.... --------_._--_ .. _-_.-._-----_.-. __ ..... _._._._-_ .. __ ._ .. _._._._. __ ._ ... _._ .. __ .. _ ... --'--'-"--... __ .. _-_ .. ---.... -.-_ .. _ ... -.-._._--_ ... _--_.-.......•......................•........................... _._. :~:::::::::=:=::::::::::::::::::::::=::::::=:::=:::=::::::::::=:::::::====:::==:::==:::::::::::::=====:::==:==:==:==:====:==:::::===:::==:==:::::==:::::::::::::::::::=:::=::::::::::::::::::::::::::::::::: ::::=:::::::::::::=::::::::::=::::::::::~: .. . ..... :.: .. :.::::::::::::::::::::::::=::::::::::::::::::::::=::'::::::::: ...... ~ ........ :.. . .: .. :.:: .. :.: .. :.: .. ::.::::::.:::::~ .. ::::::.:.:::::::::::::::::::::::::.:.:::::=:::=:::::::.:.:.:=:::~........... :::::::::::::::::::::::::::::::::::::::::::.:::::::::::::::::: m ro ~.OOE-14 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ ~ 1.00E-15 _~=.:==.~::':=::::::::=-._. :~~:~ ............................................................... - 1 .00 E -16 ::::--=====-=::::-_.::::-_ =¥=~:::::=~==::::::::::::::::::::::::::::::=:::::=~::::::::::::::::::::=:::::==! .....••....•.......••.... _ ........ _ ... _ ... _ ........ -.......................................................... --..... _ ... _ ... - .. __ .. _----_. __ . __ .. _--_. __ . __ .. _ .. _-_ ... _---_ .. _._ .. -............... _._ ..... _._ ...... _ ............... _ .. _ ..... _ ...... _ . ..................... _ ....... 1.00E-17 I T""" N ('I) ~ L() co I"-co 0") 0 T""" N ('I) ~ L() co I"-co 0") 0 T""" N ('I) ~ L() co I"-co 0") 0 co co co co co co co co co 0") 0") 0") 0") 0") 0") 0") 0") 0") 0") 0 0 0 0 0 0 0 0 0 0 T""" T""" I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. a.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) 1.00E-11 Effluent Concentration Limit = 2E-14 uCi/ml ALARA Goal = 5E-13 uCi/ml Pre 1994 MPC Limit = 8E-14uCi/ml BHV-2 Thorium-230 Concentrations (uCi/ml) 1.00E-12 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1 , tn~~4 ~~~~~~~~---=~~=~~=~-~==~===_~= ~~~~~ s ________ _____ ,=oc __ ._ .. ___ .... _:~'::~_,::::,,':::=----OJ --"cc . __ . __ ._ ... ___ . __________ _ :4_00E-15 ' ____ =~=--_________ _ .......................... _. 1_ OOE-16 ~-----"===-_-=-=~-:::::~_._. ___ . ___ ._._. __ . __ ._._. _____ . _____ _ ---------_._-----._--. __ .-.- ~ 1.00E-17 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-18 T""" N C"') "'¢ L() <.0 "-ex> 0"> 0 T""" N C"') "'¢ L() <.0 "-ex> 0"> 0 T""" N C"') "'¢ L() <.0 "-ex> 0"> 0 ex> ex> ex> ex> ex> ex> ex> ex> ex> 0"> 0"> 0"> 0"> 0"> 0"> 0"> 0"> 0"> 0"> 0 0 0 0 0 0 0 0 0 0 T""" T""" I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) 1.00E-11 Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml BHV-2 Radium-226 Concentrations (uCi/ml) 1.00E-12[ .. _ __.. ~ j ._ .. _-------------_.-. - --. '--'----. -. -._-----.. _---_ .... _------. -_.-.---- -.. --_._-._-_. __ .... , .. __ ._--... -.......... __ ...... _ ................ _ ................ ,_ ............................ ,_ ...................... _ .......................................................................................................................................................................... . ;:::::::::::::::::::::::::::::::::::::::::::::=::::::::::::::::::::::::::::::::::::::::==~:::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::.~::::::::::;:================::====================:===:::::::::::=:::::=::=:::=::==:=:::::::::====::==========::==:::::===::::::::::::::::=:::::::====:::::::::===::::::::::::: 1.00E-13 m ro \ '- ~.OOE-14 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ -J ---- 1.00E-15 1.00E-16 1.00E-17 T"" N C"') -.::t L() co co co co co co co I I I I I I c.. c.. c.. c.. c.. c.. Q) Q) Q) Q) Q) Q) C/) C/) C/) C/) C/) C/) I'-co 0') 0 co co co 0') I I I I c.. c.. c.. c.. Q) Q) Q) Q) C/) C/) C/) C/) T"" N C"') 0') 0') 0') I I I c.. c.. c.. Q) Q) Q) C/) C/) C/) . __ ... __ ... __ ... __ ... __ .•....•. __ ............ __ ...... -.-.. -.-....... -... . ........ -.... -.........•..•........•...................•. -.........•.•.....•........ _ ... -....................................... - ................. -.... _ .. -•..... _-.. -.-..•..•..•....••.............••..•.........••.........• '-' -.::t L() co I'-co 0') 0 T"" N C"') -.::t L() co I'-co 0') 0 0') 0') 0') 0') 0') 0') 0 0 0 0 0 0 0 0 0 0 T"" I I I I I I I I I I I I I I I I I c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) C/) T"" I c.. Q) C/) 1.00E-11 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCilml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1 E-12 uCi/ml BHV-2 Lead-210 Concentrations (uCi/ml) I , 1 .00 E -12 r~~~~~~~~~~~~~~~~~;;~~~~~~~~~~~·=.~~~~~~~~~~~~~=.~=.~~~~~~~~~~~~~~tt=~~~=====~===-============~:::=-~==-====~:==~====~=~========~:~~=:~~=~=~:~~:~~:~~=~=~=~:~~:::::=~:::~:~~~:~=~:=:~::=~~:~:=1 I 1.00E-13 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 'W' n ~ --~-... .._----------. ctl ~.00E-14 C) ............................. - o ....J -.---.-.--.---------------.------......... -_. __ . __ .-._._ ..... _. __ . __ .-._.---_.-_ .•. _._-.. _--- -------_._ .... _--_._ .... _--_._ .... _- l 1.00E-15 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-16 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-17 T""" N ("") ooq-L!) co I"---00 0'> 0 T""" N ("") ooq-L!) co I"---00 0'> 0 T""" N ("") ooq-L!) co I"---00 0'> 0 00 00 00 00 00 00 00 00 00 0'> 0'> 0'> 0'> 0'> 0'> 0'> 0'> 0'> 0'> 0 0 0 0 0 0 0 0 0 0 T""" T""" I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) en en en en en en en en en en en en en en en en en en en en en en en en en en en en en en en TAB 3 BHV-3 AIR SAMPLING GRAPHS AND DATA TABLE i I'·· .' Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-3U Effluent Concentration Limit = 2E-14 uCi/ml BHV-3T Effluent Concentration Limit = 9E-13 uCi/ml BHV-3R Effluent Concentration Limit = 6E-13 uCi/ml BHV-3PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 1.74E-1S S.00E-12 1.2SE-12 9.02E-16 8.00E-14 2.00E-14 2.87E-16 2.00E-12 S.OOE-13 1.S4E-14 4.00E-12 1.00E-12 12/14/1981 1.59E-1S S.00E-12 l.2SE-12 S.03E-16 8.00E-14 2.00E-14 1.30E-16 2.00E-12 S.OOE-13 2.2SE-14 4.00E-12 1.00E-12 3/29/1982 3.76E-16 S.00E-12 1.2SE-12 S.2SE-16 8.00E-14 2.00E-14 4.08E-16 2.00E-12 S.OOE-13 1.96E-14 4.00E-12 1.00E-12 6/30/1982 3.83E-16 S.00E-12 l.2SE-12 2.16E-16 8.00E-14 2.00E-14 1.4lE-1S 2.00E-12 S.OOE-13 2.40E-14 4.00E-12 1.00E-12 9/27/1982 S.9SE-16 S.00E-12 1.2SE-12 1.44E-1S 8.00E-14 2.00E-14 S.36E-16 2.00E-12 S.OOE-13 1.43E-14 4.00E-12 1.00E-12 1/3/1983 2.0SE-16 S.00E-12 1.2SE-12 1.23E-16 8.00E-14 2.00E-14 1.10E-16 2.00E-12 S.OOE-13 3.01E-14 4.00E-12 1.00E-12 4/4/1983 1.00E-16 S.00E-12 1.2SE-12 6.94E-17 8.00E-14 2.00E-14 6.11E-17 2.00E-12 S.OOE-13 1.39E-14 4.00E-12 1.00E-12 6/30/1983 3.06E-16 S.00E-12 1.2SE-12 9.S9E-17 8.00E-14 2.00E-14 2.08E-16 2.00E-12 S.OOE-13 1.70E-14 4.00E-12 1.00E-12 10/3/1983 1.9lE-16 S.00E-12 1.2SE-12 3.0SE-16 8.00E-14 2.00E-14 2.79E-16 2.00E-12 S.OOE-13 1.76E-14 4.00E-12 1.00E-12 1/3/1984 3.0lE-16 S.00E-12 1.2SE-12 9.S1E-17 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 9.17E-1S 4.00E-12 1.00E-12 4/2/1984 8.22E-16 S.00E-12 1.2SE-12 7.S2E-16 8.00E-14 2.00E-14 S.20E-17 2.00E-12 S.OOE-13 3.47E-14 4.00E-12 1.00E-12 7/2/1984 S.29E-16 S.00E-12 l.2SE-12 6.18E-16 8.00E-14 2.00E-14 1.40E-16 2.00E-12 S.OOE-13 1.32E-14 4.00E-12 1.00E-12 10/1/1984 1.74E-16 S.00E-12 l.2SE-12 7.10E-17 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 1.08E-14 4.00E-12 1.00E-12 1/2/1985 1.00E-17 S.00E-12 l.2SE-12 7.10E-17 8.00E-14 2.00E-14 7.80E-17 2.00E-12 S.OOE-13 2.73E-14 4.00E-12 1.00E-12 4/1/1985 1.00E-16 S.00E-12 1.2SE-12 2.76E-16 8.00E-14 2.00E-14 4.10E-17 2.00E-12 S.OOE-13 1.12E-14 4.00E-12 1.00E-12 7/1/1985 1.04E-16 S.00E-12 1.2SE-12 1.00E-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 1.64E-14 4.00E-12 1.00E-12 9/30/1985 1.00E-16 S.00E-12 1.2SE-12 1.00E-1S 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 1.73E-14 4.00E-12 1.00E-12 1/2/1986 1.03E-1S S.00E-12 1.2SE-12 3.17E-16 8.00E-14 2.00E-14 l.2SE-16 2.00E-12 S.OOE-13 1.21E-17 4.00E-12 1.00E-12 4/1/1986 8.04E-16 S.OOE-12 1.2SE-12 1.93E-17 8.00E-14 2.00E-14 1.S4E-16 2.00E-12 S.OOE-13 1.69E-14 4.00E-12 1.00E-12 6/30/1986 4.29E-16 S.00E-12 1.2SE-12 1.77E-16 8.00E-14 2.00E-14 2.83E-16 2.00E-12 S.OOE-13 1.97E-14 4.00E-12 1.00E-12 10/27/1986 6.4SE-16 S.00E-12 1.2SE-12 9.89E-17 8.00E-14 2.00E-14 4.16E-1S 2.00E-12 S.OOE-13 1.64E-14 4.00E-12 1.00E-12 12/15/1986 1.31E-16 S.00E-12 1.2SE-12 O.OOE+OO 8.00E-14 2.00E-14 4.16E-17 2.00E-12 S.OOE-13 4.60E-1S 4.00E-12 1.00E-12 3/16/1987 2.0lE-16 S.00E-12 1.2SE-12 1.20E-16 8.00E-14 2.00E-14 S.73E-17 2.00E-12 S.OOE-13 1.60E-14 4.00E-12 1.00E-12 5/11/1987 2.16E-16 S.00E-12 1.2SE-12 1.96E-16 8.00E-14 2.00E-14 7.38E-17 2.00E-12 S.OOE-13 1.S9E-14 4.00E-12 1.00E-12 9/9/1987 2.4lE-16 S.00E-12 1.2SE-12 2.18E-16 8.00E-14 2.00E-14 3.S2E-17 2.00E-12 S.OOE-13 1.46E-14 4.00E-12 1.00E-12 11/2/1987 2.44E-16 S.00E-12 l.2SE-12 2.32E-16 8.00E-14 2.00E-14 2.37E-17 2.00E-12 S.OOE-13 2.48E-14 4.00E-12 1.00E-12 2/16/1988 8.08E-16 S.00E-12 l.2SE-12 2.SSE-16 8.00E-14 2.00E-14 3.42E-16 2.00E-12 S.OOE-13 S.61E-14 4.00E-12 1.00E-12 5/18/1988 1.14E-16 S.00E-12 l.2SE-12 4.14E-17 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 1.20E-14 4.00E-12 1.00E-12 8/15/1988 2.08E-16 S.00E-12 1.2SE-12 3.06E-16 8.00E-14 2.00E-14 3.6SE-17 2.00E-12 S.OOE-13 1.36E-14 4.00E-12 1.00E-12 11/14/1988 4.21E-16 S.00E-12 1.2SE-12 2.93E-16 8.00E-14 2.00E-14 1.09E-16 2.00E-12 S.OOE-13 2.48E-14 4.00E-12 1.00E-12 2/13/1989 4.4SE-16 S.00E-12 1.2SE-12 4.78E-17 8.00E-14 2.00E-14 2.47E-17 2.00E-12 S.OOE-13 3.34E-14 4.00E-12 1.00E-12 5/15/1989 1.0SE-16 S.00E-12 1.2SE-12 1.00E-16 8.00E-14 2.00E-14 2.4SE-17 2.00E-12 S.OOE-13 6.S6E-1S 4.00E-12 1.00E-12 8/14/1989 1.31E-16 S.00E-12 1.2SE-12 S.8SE-17 8.00E-14 2.00E-14 3.97E-17 2.00E-12 S.OOE-13 6.7SE-1S 4.00E-12 1.00E-12 11/13/1989 1.67E-16 S.00E-12 l.2SE-12 3.87E-17 8.00E-14 2.00E-14 8.03E-17 2.00E-12 S.OOE-13 1.69E-14 4.00E-12 1.00E-12 2/12/1990 4.43E-16 S.00E-12 1.2SE-12 1.00E-16 8.00E-14 2.00E-14 3.S0E-17 2.00E-12 S.OOE-13 2.37E-14 4.00E-12 1.00E-12 5/14/1990 3.84E-16 S.00E-12 l.2SE-12 2.S4E-16 8.00E-14 2.00E-14 1.02E-16 2.00E-12 S.OOE-13 1.68E-14 4.00E-12 1.00E-12 8/13/1990 7.27E-17 S.00E-12 1.2SE-12 2.87E-16 8.00E-14 2.00E-14 l.2lE-17 2.00E-12 S.OOE-13 7.86E-1S 4.00E-12 1.00E-12 11/12/1990 1.84E-16 S.00E-12 1.2SE-12 1.34E-16 8.00E-14 2.00E-14 8.S3E-17 2.00E-12 S.OOE-13 2.01E-14 4.00E-12 1.00E-12 2/11/1991 4.66E-17 S.00E-12 1.2SE-12 8.48E-16 8.00E-14 2.00E-14 1.94E-17 2.00E-12 S.OOE-13 3.69E-14 4.00E-12 1.00E-12 5/13/1991 S.OSE-17 S.00E-12 1.2SE-12 7.40E-17 8.00E-14 2.00E-14 7.00E-18 2.00E-12 S.OOE-13 1.50E-14 4.00E-12 1.00E-12 8/12/1991 7.14E-17 S.00E-12 1.2SE-12 6.22E-17 8.00E-14 2.00E-14 7.9SE-17 2.00E-12 S.OOE-13 1.77E-14 4.00E-12 1.00E-12 11/11/1991 1.41E-17 S.00E-12 1.2SE-12 2.19E-18 8.00E-14 2.00E-14 2.7SE-17 2.00E-12 S.OOE-13 1.18E-14 4.00E-12 1.00E-12 2/10/1992 8.12E-17 S.OOE-12 1.2SE-12 2.3SE-17 8.00E-14 2.00E-14 2.76E-18 2.00E-12 S.OOE-13 3.S7E-14 4.00E-12 1.00E-12 5/11/1992 9.18E-17 S.OOE-12 1.2SE-12 S.80E-17 8.00E-14 2.00E-14 3.36E-17 2.00E-12 S.OOE-13 1.28E-14 4.00E-12 1.00E-12 8/10/1992 2.00E-18 S.00E-12 1.2SE-12 4.19E-17 8.00E-14 2.00E-14 2.00E-18 2.00E-12 S.OOE-13 1.S9E-14 4.00E-12 1.00E-12 11/9/1992 4.00E-17 S.00E-12 l.2SE-12 2.68E-17 8.00E-14 2.00E-14 1.07E-17 2.00E-12 S.OOE-13 1.8lE-14 4.00E-12 1.00E-12 2/9/1993 7.94E-17 S.00E-12 1.2SE-12 1.00E-16 8.00E-14 2.00E-14 1.09E-16 2.00E-12 S.OOE-13 2.69E-14 4.00E-12 1.00E-12 5/10/1993 1.60E-17 S.00E-12 1.2SE-12 S.07E-17 8.00E-14 2.00E-14 7.64E-17 2.00E-12 S.OOE-13 1.26E-14 4.00E-12 1.00E-12 8/10/1993 6.00E-17 S.00E-12 1.2SE-12 6.00E-18 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 1.S0E-14 4.00E-12 1.00E-12 11/8/1993 1.00E-16 S.00E-12 1.2SE-12 1.00E-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 2.10E-14 4.00E-12 1.00E-12 2/7/1994 1.6lE-16 S.00E-12 1.2SE-12 1.00E-16 8.00E-14 2.00E-14 2.22E-16 2.00E-12 S.OOE-13 2.23E-14 4.00E-12 1.00E-12 5/9/1994 2.77E-16 S.00E-12 1.2SE-12 2.80E-17 8.00E-14 2.00E-14 8.37E-18 2.00E-12 S.OOE-13 1.40E-14 4.00E-12 1.00E-12 8/9/1994 7.39E-17 S.00E-12 1.2SE-12 1.00E-16 8.00E-14 2.00E-14 1.14E-16 2.00E-12 S.OOE-13 1.00E-16 4.00E-12 1.00E-12 11/7/1994 9.0SE-17 S.00E-12 1.2SE-12 1.00E-16 8.00E-14 2.00E-14 1.00E-16 2.00E-12 S.OOE-13 1.00E-16 4.00E-12 1.00E-12 2/7/1995 7.99E-17 9.00E-14 2.2SE-14 9.60E-17 2.00E-14 S.00E-1S 9.60E-17 9.00E-13 2.2SE-13 9.0SE-1S 6.00E-13 1.S0E-13 5/9/1995 9.40E-17 9.00E-14 2.2SE-14 9.80E-17 2.00E-14 S.00E-1S 8.60E-17 9.00E-13 2.2SE-13 2.88E-1S 6.00E-13 1.S0E-13 8/9/1995 7.30E-17 9.00E-14 2.2SE-14 9.20E-17 2.00E-14 S.00E-1S 4.40E-17 9.00E-13 2.2SE-13 1.96E-1S 6.00E-13 1.S0E-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-3U Effluent Concentration Limit = 2E-14 uCi/ml BHV-3T Effluent Concentration Limit = 9E-13 uCi/ml BHV-3R Effluent Concentration Limit = 6E-13 uCi/ml BHV-3PB ALARAGoal = 2.2SE-14 uCi/ml ALARA Goal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA 11/11/1995 3.16E-16 9.00E-14 2.2sE-14 l.3IE-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2sE-13 1.9IE-14 6.00E-13 l.sOE-13 2/5/1996 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 l.sOE-13 5/6/1996 1.3IE-16 9.00E-14 2.2sE-14 l.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 l.s3E-14 6.00E-13 l.sOE-13 8/5/1996 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 l.31E-14 6.00E-13 l.sOE-13 11/6/1996 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2sE-13 1.9IE-14 6.00E-13 l.sOE-13 2/6/1997 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 l.sOE-13 5/5/1997 1.31E-16 9.00E-14 2.2sE-14 l.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 l.s3E-14 6.00E-13 l.sOE-13 8/11/1997 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 l.31E-14 6.00E-13 l.sOE-13 1/5/1998 3.16E-16 9.00E-14 2.2sE-14 l.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2sE-13 1.9IE-14 6.00E-13 l.sOE-13 4/28/1998 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.l8E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 l.sOE-13 7/31/1998 1.3IE-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 l.s3E-14 6.00E-13 l.sOE-13 9/28/1998 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 l.31E-14 6.00E-13 l.sOE-13 12/28/1998 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 1.s0E-13 3/29/1999 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 l.sOE-13 7/3/1999 l.31E-16 9.00E-14 2.2sE-14 l.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 l.s3E-14 6.00E-13 l.sOE-13 9/27/1999 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 l.31E-14 6.00E-13 l.sOE-13 12/28/1999 3.16E-16 9.00E-14 2.2sE-14 l.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 l.sOE-13 3/28/2000 3.4IE-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.l8E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 l.sOE-13 6/26/2000 1.3IE-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 1.s3E-14 6.00E-13 1.s0E-13 9/26/2000 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 1.S0E-13 12/26/2000 3.16E-16 9.00E-14 2.2SE-14 l.3IE-16 2.00E-14 S.00E-1S 6.S8E-17 9.00E-13 2.2SE-13 1.9IE-14 6.00E-13 l.SOE-13 3/26/2001 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.00E-1S 1.18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 l.SOE-13 7/2/2001 1.31E-16 9.00E-14 2.2sE-14 l.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 l.s3E-14 6.00E-13 l.SOE-13 9/24/2001 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1s 3.99E-16 9.00E-13 2.2sE-13 l.31E-14 6.00E-13 1.s0E-13 12/31/2001 3.16E-16 9.00E-14 2.2SE-14 1.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 1.s0E-13 4/1/2002 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 s.OOE-ls 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 l.SOE-13 7/1/2002 1.31E-16 9.00E-14 2.2SE-14 l.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 l.S3E-14 6.00E-13 l.sOE-13 9/30/2002 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2SE-13 l.3IE-14 6.00E-13 l.SOE-13 12/30/2002 3.16E-16 9.00E-14 2.2SE-14 l.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2SE-13 1.91E-14 6.00E-13 l.SOE-13 3/31/2003 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 s.OOE-ls 1.l8E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 1.s0E-13 6/30/2003 l.31E-16 9.00E-14 2.2sE-14 1.39E-16 2.00E-14 s .OOE-ls 1.82E-16 9.00E-13 2.2sE-13 1.s3E-14 6.00E-13 l.sOE-13 9/29/2003 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1s 3.99E-16 9.00E-13 2.2SE-13 1.3IE-14 6.00E-13 l.sOE-13 12/29/2003 3.16E-16 9.00E-14 2.2sE-14 l.3IE-16 2.00E-14 s.OOE-lS 6.S8E-17 9.00E-13 2.2SE-13 1.9IE-14 6.00E-13 l.SOE-13 3/29/2004 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s .OOE-ls 1.l8E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 l.SOE-13 6/27/2004 1.3IE-16 9.00E-14 2.2SE-14 1.39E-16 2.00E-14 S.00E-1s 1.82E-16 9.00E-13 2.2SE-13 l.S3E-14 6.00E-13 l.SOE-13 9/27/2004 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2SE-13 l.31E-14 6.00E-13 l.sOE-13 12/27/2004 3.16E-16 9.00E-14 2.2SE-14 l.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 l.SOE-13 3/28/200S 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.00E-1S 1.18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 l.sOE-13 6/29/2005 1.31E-16 9.00E-14 2.2sE-14 l.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 1.s3E-14 6.00E-13 l.SOE-13 9/26/2005 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 1.3IE-14 6.00E-13 1.50E-13 1/3/2006 3.16E-16 9.00E-14 2.2SE-14 l.31E-16 2.00E-14 S.00E-1s 6.S8E-17 9.00E-13 2.2SE-13 1.91E-14 6.00E-13 l.SOE-13 4/3/2006 3.4IE-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 S.00E-1S 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 l.sOE-13 7/3/2006 l.31E-16 9.00E-14 2.2sE-14 l.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 l.S3E-14 6.00E-13 l.sOE-13 10/2/2006 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 1.S0E-13 1/1/2006 3.16E-16 9.00E-14 2.2SE-14 1.31E-16 2.00E-14 S.00E-1S 6.S8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 l.SOE-13 4/2/2007 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 l.sOE-13 7/2/2007 1.31E-16 9.00E-14 2.2sE-14 l.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2SE-13 l.s3E-14 6.00E-13 l.sOE-13 9/30/2007 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2SE-13 l.31E-14 6.00E-13 l.sOE-13 12/31/2007 3.16E-16 9.00E-14 2.2SE-14 1.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 1.S0E-13 3/31/2008 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 s.OOE-ls 1.l8E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 l.sOE-13 6/30/2008 l.31E-16 9.00E-14 2.2SE-14 1.39E-16 2.00E-14 S.00E-1s 1.82E-16 9.00E-13 2.2SE-13 l.S3E-14 6.00E-13 1.S0E-13 9/30/2008 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 S.00E-1s 3.99E-16 9.00E-13 2.2sE-13 1.31E-14 6.00E-13 1.s0E-13 12/31/2008 3.16E-16 9.00E-14 2.2SE-14 l.3IE-16 2.00E-14 S.00E-1s 6.S8E-17 9.00E-13 2.2SE-13 1.9IE-14 6.00E-13 l.SOE-13 3/15/2009 3.41E-16 9.00E-14 2.2sE-14 2.26E-16 2.00E-14 S.00E-1s 1.18E-16 9.00E-13 2.2sE-13 2.69E-14 6.00E-13 l.sOE-13 6/15/2009 1.3IE-16 9.00E-14 2.2sE-14 l.39E-16 2.00E-14 s.OOE-ls 1.82E-16 9.00E-13 2.2sE-13 l.s3E-14 6.00E-13 l.sOE-13 9/15/2009 3.00E-16 9.00E-14 2.2sE-14 3.43E-16 2.00E-14 s.OOE-ls 3.99E-16 9.00E-13 2.2sE-13 l.31E-14 6.00E-13 l.sOE-13 12/15/2009 3.16E-16 9.00E-14 2.2sE-14 1.31E-16 2.00E-14 s.OOE-ls 6.s8E-17 9.00E-13 2.2sE-13 1.91E-14 6.00E-13 1.s0E-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-3U Effluent Concentration Limit = 2E-14 uCi/ml BHV-3T Effluent Concentration Limit = 9E-13 uCi/ml BHV-3R Effluent Concentration Limit = 6E-13 uCi/ml BHV-3PB ALARA Goal = 2.2SE-14 uCi/ml ALARA Goal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA Conc EFC EFCA 3/31/2010 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.00E-1S l.18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 l.SOE-13 6/30/2010 l.31E-16 9.00E-14 2.2SE-14 1.39E-16 2.00E-14 S.00E-1S l.82E-16 9.00E-13 2.2SE-13 l.S3E-14 6.00E-13 l.SOE-13 9/30/2010 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2SE-13 l.31E-14 6.00E-13 l.SOE-13 12/31/2010 3.16E-16 9.00E-14 2.2SE-14 l.31E-16 2.00E-14 S.00E-1S 6.S8E-17 9.00E-13 2.2SE-13 l.9IE-14 6.00E-13 l.SOE-13 4/4/2011 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.00E-1S 1.18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 l.SOE-13 7/4/2011 1.31E-16 9.00E-14 2.2SE-14 1.39E-16 2.00E-14 S.00E-1S l.82E-16 9.00E-13 2.2SE-13 l.53E-14 6.00E-13 l.SOE-13 10/3/2011 3.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 3.99E-16 9.00E-13 2.2SE-13 l.31E-14 6.00E-13 l.SOE-13 1/3/2012 3.16E-16 9.00E-14 2.2SE-14 1.3IE-16 2.00E-14 S.00E-1S 6.S8E-17 9.00E-13 2.2SE-13 l.91E-14 6.00E-13 l.SOE-13 4/3/2012 3.41E-16 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.00E-1S l.18E-16 9.00E-13 2.2SE-13 2.69E-14 6.00E-13 1.S0E-13 7/2/2012 l.31E-16 9.00E-14 2.2SE-14 1.39E-16 2.00E-14 S.00E-1S l.82E-16 9.00E-13 2.2SE-13 1.S3E-14 6.00E-13 l.SOE-13 -E =::::: U :l - N T""" I W o o ('I') T""" I W o o 1 ~ 1 ........... 1 I I" ~ 1 ·;I L",; I..i..~ , IT II I! I ! I ! I ! .. 1""-1 -~I "'d" T""" I W o o LO T""" I W 0 ~ T""" (ele~s 601) co T""" I W 0 ~ T""" ~ ~-des o~-des 60-deS go-des La-des go-des so-des va-des 0 T""" £O-deS N I "'C co la-des Q) .....J ~o-des t oo-des co N N 66-deS I E .~ 96-deS "'C co 0:: L6-deS t 96-deS 0 S6-deS ('I') N I v6-deS E :::J ·c 0 £6-deS ...c ; r- ! I! l6-de S t !! ! i I , . I , ! .... ~6-des ro L.. 06-deS :::J ro z 69-deS E :::J gg-des ·c co L.. => L9-deS t gg-deS Sg-deS vg-des £g-deS 19-deS ~g-des I'--co T""" T""" I I W W 0 0 ~ ~ T""" T""" 1.00E-11 Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml BHV-3 Uranium-Natural Concentrations (uCi/ml) 1.00E-12 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ ----------------- - - - ----- --- --- - - - - - - - - -.-.-.-. __ . __ ...... _--. __ ._---... _----. __ .-..... _-.-._ ... _-" .. -.-.... -._ ........ _ .............. _--_ ........ __ . __ ........ _ ... _ ............. _ ...... __ ... __ .............. __ ..•..•.............•.... __ .. _._--_ .. . 1.00E-13 lu .... ··t ~ ,.t.OOE-14 t - --- ----- ------.---------.--------.----...... ---... -... -.. -.-.~ "* ~~~~~----~-~~-~~~~-----~-~~~~-~~-~~~~--~~~~~-~~-~~-~--~~~~~~~~-=-~~~-=-~-~~~-~-~-~-~~-==-~-~~~~~~-=-~~~~~~~~~~:~~~~==~~~ ... ~~~::~==~~:::::=~:~~~~-~~~~=~=~=~~~~:::~~~::::::::~~:~::::::::=.:::~~::::::::~:::=--... -... -.-.. (.) CJ) 0) o .....J '"f.OOE-15 1.00E-16 ~ .. . __ .......... _--_ ... _._ .. _._. . __ . __ ._ ... __ . __ ._._-_. __ . __ . --------_._------------------=.::..::..:..-=--.....::-----------------------===----------- 1.00E-17 -.--... -......... .. -~- -==-~~~~~~~~~~~~~~~~~~~~ -===-~~~=~~~~~~~~==~~=.;~~~~~~~=.~~=.:--=.~~~;~;~~=~~-==-======-~~~~=--=. -------- 1.00E-18 ~ N ('t) ~ L(,) co "-co 0) 0 ~ N ('t) ~ L(,) co "-co 0) 0 ~ N ('t) ~ L(,) co "-co 0) 0 co co co co co co co co co 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0 0 0 0 0 0 0 0 0 0 ~ ~ I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CJ) CJ) CJ) CJ) CJ) CJ) CJ) en CJ) CJ) CJ) CJ) CJ) en en CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) -E :::: o :l -en c o ~ e ~ c Cl) (.) c o o o M N I E :l ".: o .c I- M ::> ::I: In T""" T""" I W o o N T""" I W o o C") T""" I W o o ~ L() T""" T""" I I W W o 0 o 0 ~ale~s 601f , .: ! • i.~· i. i .! ......... ~ . : ~J , ~~.r!""· ~~ !i!! I 1 ! co T""" I W o o ~ ~-das o~-das 60-daS go-das LO-daS go-das go-das Po-das £O-daS lO-daS ~o-das OO-daS 66-daS 96-daS L6-daS 96-daS 96-daS P6-daS £6-daS l6-daS ~6-das 06-daS 69-daS gg-daS L9-daS gg-daS gg-daS pg-daS £g-daS 19-daS ~g-das I'--CO T""" T""" I I W W 0 0 ~ ~ T""" T""" 1.00E-11 Effluent Concentration Limit = 6E-13 uCilml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1 E-12 uCi/ml BHV-3 Lead-210 Concentrations (uCi/ml) 1 1 .00 E -1 2 I~~~::=~~~=~::=.~~::=.~~~~::~::=~=.~~::~~~~~~~::=.~~::=~::=.~::=~::=.=~::=~::=.~=.~~===~::=.~::~=.=.=.==.==~::=.=~==.l'==============~====~=============~=:::==============:~===:::~:~=:::=:=~:=====~===:=::===:=:====:~:~::=~===::====::=:===::=:=:::=::~=:::::=::=::.===:::==:=::=:.~~~l , I 1.00E-13 F~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ • . ....................................................................................................................................................................................................................... ············1 Q) ro c?j .00E-14 0> ..... -.-... -.. -.-...... ---.-o --------------------------------------.. --.---... ---...... --... -.. -... -........ -. . .................................................... -... . ---1 ----------------------------------------------------.-----------.----------------.---.--.------... --.--.----... -.------.. ............ --_. __ . __ ... _._-_ ... __ ... _._ ... _--_ ... _ ... _._ ........ --.................................. -.............•.•..•............. -... . . _--_. __ . __ . __ ._----------_._------------------_._-_ .. ---_._-----_ .. _-- ... 1.00E-15 ~~~~~~€~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-16 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-17 I • T""" N C") ~ LO co """ co 0) 0 T""" N C") ~ LO co """ co 0) 0 T""" N C") ~ LO co """ co 0) 0 co co co co co co co co co 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0 0 0 0 0 0 0 0 0 0 T""" T""" I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) TAB 4 BHV-4 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-4U Effluent Concentration Limit = 2E-14 uCi/ml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = lE-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 s.20E-1s s.OOE-12 l.2sE-12 2.93E-1s 8.00E-14 2.00E-14 2.74E-1s 2.00E-12 s.OOE-13 l.84E-14 4.00E-12 1.00E-12 12/14/1981 4.s3E-1s s.00E-12 l.2sE-12 l.78E-1s 8.00E-14 2.00E-14 2.29E-1s 2.00E-12 s.OOE-13 2.s4E-14 4.00E-12 1.00E-12 3/29/1982 l.06E-1s s.00E-12 l.2sE-12 l.42E-14 8.00E-14 2.00E-14 l.07E-1s 2.00E-12 S.OOE-13 2.31E-14 4.00E-12 l.OOE-12 6/30/1982 6.03E-1S S.00E-12 l.2SE-12 l.S7E-14 8.00E-14 2.00E-14 2.62E-1s 2.00E-12 S.OOE-13 2.2SE-14 4.00E-12 1.00E-12 9/27/1982 l.26E-14 s.00E-12 l.2sE-12 7.s8E-16 8.00E-14 2.00E-14 s.3sE-1s 2.00E-12 S.OOE-13 2.68E-14 4.00E-12 l.00E-12 1/3/1983 4.33E-1s s.00E-12 l.2sE-12 6.s2E-16 8.00E-14 2.00E-14 6.04E-16 2.00E-12 s.OOE-13 2.s7E-14 4.00E-12 l.OOE-12 4/4/1983 1.2sE-1s s.00E-12 l.2sE-12 7.17E-16 8.00E-14 2.00E-14 6.76E-16 2.00E-12 s.OOE-13 2.00E-14 4.00E-12 1.00E-12 6/30/1983 3.73E-16 s.00E-12 l.2SE-12 9.43E-16 8.00E-14 2.00E-14 4.13E-16 2.00E-12 S.OOE-13 l.20E-14 4.00E-12 1.00E-12 10/3/1983 2.s4E-16 s.00E-12 1.2SE-12 1.s1E-16 8.00E-14 2.00E-14 2.6sE-16 2.00E-12 s.OOE-13 2.s0E-14 4.00E-12 l.OOE-12 1/3/1984 2.76E-1s S.00E-12 l.2SE-12 l.60E-16 8.00E-14 2.00E-14 l.OSE-16 2.00E-12 S.OOE-13 l.s9E-16 4.00E-12 l.00E-12 4/2/1984 4.27E-16 s.00E-12 l.2sE-12 2.33E-16 8.00E-14 2.00E-14 6.28E-16 2.00E-12 S.OOE-13 3.67E-14 4.00E-12 l.OOE-12 7/2/1984 2.s7E-1s s.00E-12 l.2sE-12 l.36E-16 8.00E-14 2.00E-14 1.11E-16 2.00E-12 s.OOE-13 1.58E-14 4.00E-12 l.OOE-12 I 10/1/1984 4.18E-16 s.00E-12 l.2SE-12 3.s4E-16 8.00E-14 2.00E-14 l.10E-17 2.00E-12 s.OOE-13 9.83E-1s 4.00E-12 l.OOE-12 1/2/1985 s.30E-17 s.00E-12 l.2sE-12 3.ssE-17 8.00E-14 2.00E-14 7.00E-18 2.00E-12 s.OOE-13 2.s7E-14 4.00E-12 l.OOE-12 4/1/1985 l.00E-16 s.00E-12 l.2SE-12 6.00E-16 8.00E-14 2.00E-14 4.3SE-17 2.00E-12 S.OOE-13 S.02E-1S 4.00E-12 1.00E-12 7/1/1985 9.36E-16 S.00E-12 l.2sE-12 2.33E-16 8.00E-14 2.00E-14 2.36E-16 2.00E-12 s.OOE-13 7.48E-1s 4.00E-12 l.00E-12 9/30/1985 1.46E-1s s.00E-12 l.2SE-12 7.69E-16 8.00E-14 2.00E-14 s.38E-16 2.00E-12 S.OOE-13 7.86E-1S 4.00E-12 l.00E-12 1/2/1986 8.40E-1s s.00E-12 l.2sE-12 7.60E-16 8.00E-14 2.00E-14 2.99E-16 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 l.OOE-12 4/1/1986 s.79E-1s s.00E-12 l.2sE-12 s.80E-16 8.00E-14 2.00E-14 l.34E-1s 2.00E-12 s.OOE-13 l.33E-14 4.00E-12 l.OOE-12 6/30/1986 s.19E-1s s.00E-12 l.2sE-12 7.83E-16 8.00E-14 2.00E-14 2.20E-1s 2.00E-12 s.OOE-13 7.14E-16 4.00E-12 l.OOE-12 10/27/1986 4.60E-1s s.00E-12 l.2sE-12 4.67E-16 8.00E-14 2.00E-14 2.37E-1s 2.00E-12 s.OOE-13 l.13E-14 4.00E-12 l.OOE-12 12/15/1986 2.7sE-1S s.00E-12 l.2sE-12 s.90E-16 8.00E-14 2.00E-14 9.39E-16 2.00E-12 s.OOE-13 l.20E-14 4.00E-12 l.OOE-12 3/16/1987 4.64E-1s s.OOE-12 l.2sE-12 l.18E-1S 8.00E-14 2.00E-14 4.97E-16 2.00E-12 S.OOE-13 s.89E-14 4.00E-12 l.00E-12 5/11/1987 4.3SE-1s s.00E-12 l.2SE-12 l.23E-14 8.00E-14 2.00E-14 1.13E-1S 2.00E-12 s.OOE-13 2.21E-14 4.00E-12 l.OOE-12 9/9/1987 6.39E-1s s.00E-12 l.2sE-12 1.50E-14 8.00E-14 2.00E-14 2.26E-1s 2.00E-12 s.OOE-13 1.57E-14 4.00E-12 l.OOE-12 11/2/1987 6.72E-1s S.00E-12 l.2sE-12 4.s3E-16 8.00E-14 2.00E-14 2.20E-1s 2.00E-12 S.OOE-13 2.ssE-14 4.00E-12 l.OOE-12 2/16/1988 l.91E-1S s.00E-12 l.2sE-12 l.3SE-14 8.00E-14 2.00E-14 4.42E-16 2.00E-12 S.OOE-13 4.44E-14 4.00E-12 1.00E-12 5/18/1988 l.78E-14 s.00E-12 l.2sE-12 4.39E-14 8.00E-14 2.00E-14 4.92E-16 2.00E-12 s.OOE-13 l.38E-14 4.00E-12 l.OOE-12 8/15/1988 7.s6E-1s S.00E-12 l.2sE-12 3.31E-14 8.00E-14 2.00E-14 1.s1E-1s 2.00E-12 S.OOE-13 l.97E-14 4.00E-12 l.OOE-12 11/14/1988 l.47E-14 S.00E-12 l.2SE-12 l.S6E-1S 8.00E-14 2.00E-14 2.S7E-1S 2.00E-12 s.OOE-13 2.12E-14 4.00E-12 l.OOE-12 2/13/1989 2.47E-1s S.00E-12 l.2sE-12 3.14E-1S 8.00E-14 2.00E-14 6.94E-16 2.00E-12 S.OOE-13 2.12E-14 4.00E-12 l.OOE-12 5/15/1989 2.s0E-16 s.00E-12 l.2sE-12 7.68E-1s 8.00E-14 2.00E-14 9.03E-16 2.00E-12 s.OOE-13 8.0sE-1S 4.00E-12 l.OOE-12 8/14/1989 6.s0E-1s s.00E-12 l.2sE-12 4.72E-1s 8.00E-14 2.00E-14 2.3sE-1s 2.00E-12 s.OOE-13 9.9sE-1s 4.00E-12 1.00E-12 11/13/1989 9.63E-1s S.00E-12 l.2sE-12 4.0sE-1s 8.00E-14 2.00E-14 4.03E-1s 2.00E-12 s.OOE-13 1.99E-14 4.00E-12 l.OOE-12 2/12/1990 8.92E-1S s.00E-12 l.2sE-12 3.S6E-1S 8.00E-14 2.00E-14 2.89E-1s 2.00E-12 s.OOE-13 2.69E-14 4.00E-12 l.OOE-12 5/14/1990 8.90E-1s S.00E-12 l.2sE-12 3.s8E-1s 8.00E-14 2.00E-14 2.33E-1S 2.00E-12 s.OOE-13 2.09E-14 4.00E-12 l.OOE-12 8/13/1990 l.92E-1S s.00E-12 l.2SE-12 l.87E-1S 8.00E-14 2.00E-14 s.06E-16 2.00E-12 s.OOE-13 8.86E-1S 4.00E-12 l.00E-12 11/12/1990 2.91E-1s s.00E-12 l.2sE-12 2.2sE-17 8.00E-14 2.00E-14 l.08E-1s 2.00E-12 s.OOE-13 2.19E-14 4.00E-12 l.00E-12 2/11/1991 l.67E-16 S.00E-12 l.2SE-12 7.89E-16 8.00E-14 2.00E-14 6.38E-17 2.00E-12 S.OOE-13 4.19E-14 4.00E-12 l.00E-12 5/13/1991 l.87E-16 S.00E-12 l.2SE-12 2.61E-1S 8.00E-14 2.00E-14 3.s4E-16 2.00E-12 S.OOE-13 1.40E-14 4.00E-12 1.00E-12 8/12/1991 4.8SE-16 s.00E-12 l.2sE-12 4.38E-16 8.00E-14 2.00E-14 l.27E-16 2.00E-12 s.OOE-13 2.20E-14 4.00E-12 l.OOE-12 11/11/1991 l.77E-16 ' S.00E-12 l.2SE-12 l.46E-16 8.00E-14 2.00E-14 3.76E-17 2.00E-12 S.OOE-13 l.1SE-14 4.00E-12 l.OOE-12 2/10/1992 l.83E-16 S.00E-12 l.2sE-12 l.9sE-1s 8.00E-14 2.00E-14 l.33E-16 2.00E-12 s.OOE-13 3.3sE-14 4.00E-12 l.00E-12 5/11/1992 4.40E-16 s.00E-12 1.2SE-12 2.s6E-16 8.00E-14 2.00E-14 4.04E-16 2.00E-12 s.OOE-13 l.41E-14 4.00E-12 l.OOE-12 8/10/1992 9.09E-17 s.00E-12 1.2sE-12 1.1sE-16 8.00E-14 2.00E-14 4.S0E-17 2.00E-12 s.OOE-13 l.s7E-14 4.00E-12 l.OOE-12 11/9/1992 2,07E-16 s,00E-12 l.2SE-12 l.00E-16 8.00E-14 2.00E-14 3.62E-17 2.00E-12 s,OOE-13 2.24E-14 4,00E-12 l.OOE-12 2/9/1993 l.73E-16 s.00E-12 l.2sE-12 2.76E-17 8.00E-14 2.00E-14 2.89E-17 2.00E-12 s.OOE-13 3.08E-14 4.00E-12 1.00E-12 5/10/1993 2.70E-17 s.00E-12 l.2sE-12 2.s0E-17 8.00E-14 2.00E-14 8.74E-17 2.00E-12 s.OOE-13 l.2sE-14 4.00E-12 l.00E-12 8/10/1993 9.00E-17 s.OOE-12 l.2sE-12 1.76E-16 8.00E-14 2.00E-14 O.OOE+OO 2.00E-12 s .OOE-13 l.sOE-14 4.00E-12 l.OOE-12 11/8/1993 l.00E-16 S.OOE-12 l.2SE-12 l.00E-16 8.00E-14 2,00E-14 6.00E-17 2.00E-12 S.OOE-13 l.7SE-14 4.00E-12 1.00E-12 2/7/1994 l.10E-16 s.00E-12 l.2sE-12 3.38E-16 8.00E-14 2.00E-14 2.21E-16 2.00E-12 s.OOE-13 3.08E-14 4.00E-12 l.OOE-12 5/9/1994 3.80E-16 S.00E-12 l.2sE-12 2.82E-16 8.00E-14 2.00E-14 3.46E-16 2.00E-12 S.OOE-13 l.73E-14 4.00E-12 l.OOE-12 8/9/1994 3.8sE-16 S.00E-12 1.2SE-12 3.s3E-16 8.00E-14 2.00E-14 l.00E-16 2.00E-12 S.OOE-13 l.00E-16 4.00E-12 l.OOE-12 11/7/1994 6.21E-17 S.00E-12 l.2sE-12 9.70E-17 8.00E-14 2.00E-14 l.96E-16 2.00E-12 S.OOE-13 l.00E-16 4.00E-12 l.OOE-12 2/7/1995 3.70E-16 9.00E-14 2.2SE-14 9.80E-17 2.00E-14 s.00E-1s 9.70E-17 9.00E-13 2.2SE-13 8.84E-1s 6.00E-13 l.sOE-13 5/9/1995 9.40E-17 9.00E-14 2.2sE-14 2,86E-16 2.00E-14 S.00E-1s 1.90E-16 9.00E-13 2.2SE-13 2.90E-1s 6.00E-13 l.sOE-13 8/9/1995 l.4sE-16 9.00E-14 2.2SE-14 2.31E-1S 2.00E-14 s.00E-1s 7.10E-17 9.00E-13 2.2SE-13 2.70E-1s 6.00E-13 l.SOE-13 I Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-4U Effluent Concentration Limit = 2E-14 uCi/ml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARA Goal = 2.2SE-13 uCi/ml ALARAGoal = l.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 11/11/1995 1.43E-14 9.00E-14 2.2sE-14 s.70E-1s 2.00E-14 s.00E-1s 2.61E-1s 9.00E-13 2.2sE-13 s.60E-1s 6.00E-13 l.sOE-13 2/5/1996 1.19E-14 9.00E-14 2.2sE-14 3.80E-16 2.00E-14 s.00E-1s 6.10E-1s 9.00E-13 2.2sE-13 6.48E-1s 6.00E-13 l.sOE-13 5/6/1996 4.ssE-16 9.00E-14 2.2sE-14 3.s7E-1s 2.00E-14 s.00E-1s 2.84E-16 9.00E-13 2.2sE-13 7.68E-1s 6.00E-13 l.sOE-13 8/5/1996 7.78E-16 9.00E-14 2.2sE-14 3.s1E-1s 2.00E-14 s.00E-1s 1.69E-16 9.00E-13 2.2sE-13 4.90E-1s 6.00E-13 1.S0E-13 11/6/1996 1.36E-1s 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 4.2lE-16 9.00E-13 2.2sE-13 1.10E-14 6.00E-13 l.sOE-13 2/6/1997 1.00E-16 9.00E-14 2.2sE-14 1.40E-16 2.00E-14 s.00E-1s 1.03E-16 9.00E-13 2.2sE-13 6.76E-1s 6.00E-13 l.sOE-13 5/5/1997 1.00E-16 9.00E-14 2.2sE-14 4.00E-16 2.00E-14 s.00E-1s 2.24E-16 9.00E-13 2.2sE-13 4.5sE-1s 6.00E-13 l.sOE-13 8/11/1997 4.74E-16 9.00E-14 2.2sE-14 9.07E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 s.ssE-1s 6.00E-13 l.sOE-13 1/5/1998 8.3lE-16 9.00E-14 2.2sE-14 4.82E-16 2.00E-14 s.00E-1s 1.77E-16 9.00E-13 2.2sE-13 s.28E-1s 6.00E-13 l.sOE-13 4/28/1998 3.32E-16 9.00E-14 2.2SE-14 4.43E-1s 2.00E-14 s.00E-1s 1.21E-16 9.00E-13 2.2sE-13 7.43E-1s 6.00E-13 l.sOE-13 7/31/1998 4.60E-16 9.00E-14 2.2sE-14 9.02E-16 2.00E-14 s.00E-1s 3.s4E-16 9.00E-13 2.2sE-13 6.91E-1s 6.00E-13 l.sOE-13 9/28/1998 4.08E-16 9.00E-14 2.2sE-14 4.93E-16 2.00E-14 s.00E-1s 2.s3E-16 9.00E-13 2.2sE-13 4.s2E-1s 6.00E-13 1.s0E-13 12/28/1998 7.72E-16 9.00E-14 2.2sE-14 3.7sE-16 2.00E-14 s.00E-1s 3.43E-16 9.00E-13 2.2sE-13 6.73E-1s 6.00E-13 1.s0E-13 3/29/1999 s .l1E-16 9.00E-14 2.2sE-14 4.70E-16 2.00E-14 s.00E-1s 3.70E-16 9.00E-13 2.2sE-13 8.96E-1s 6.00E-13 l.sOE-13 7/3/1999 s.90E-16 9.00E-14 2.2sE-14 9.89E-16 2.00E-14 s.00E-1s 1.28E-16 9.00E-13 2.2sE-13 6.40E-1s 6.00E-13 l.sOE-13 9/27/1999 1.70E-1s 9.00E-14 2.2sE-14 7.s0E-16 2.00E-14 s.00E-1s 4.61E-16 9.00E-13 2.2sE-13 7.86E-1s 6.00E-13 l.sOE-13 12/28/1999 1.03E-1s 9.00E-14 2.2sE-14 7.s0E-16 2.00E-14 s.00E-1s 2.43E-16 9.00E-13 2.2sE-13 6.42E-1s 6.00E-13 l.sOE-13 3/27/2000 1.00E-16 9.00E-14 2.2sE-14 2.13E-16 2.00E-14 s.00E-1s 2.20E-16 9.00E-13 2.2sE-13 s.61E-1s 6.00E-13 1.s0E-13 6/26/2000 1.7sE-16 9.00E-14 2.2sE-14 3.08E-16 2.00E-14 s.00E-1s 1.11E-16 9.00E-13 2.2sE-13 3.92E-1s 6.00E-13 1.s0E-13 9/26/2000 3.6sE-16 9.00E-14 2.2sE-14 2.0lE-16 2.00E-14 s.00E-1s 2.24E-16 9.00E-13 2.2sE-13 7.79E-1s 6.00E-13 1.s0E-13 12/26/2000 2.27E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 S.00E-1s 4.3sE-16 9.00E-13 2.2sE-13 8.4sE-1S 6.00E-13 l.sOE-13 3/26/2001 1.4sE-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 6.37E-1s 6.00E-13 l.sOE-13 7/2/2001 1.00E-16 9.00E-14 2.2sE-14 1.0sE-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 6.99E-1s 6.00E-13 l.sOE-13 9/24/2001 1.91E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 2.01E-16 9.00E-13 2.2sE-13 8.04E-1s 6.00E-13 1.s0E-13 12/31/2001 l.38E-16 9.00E-14 2.2sE-14 2.0sE-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.83E-1s 6.00E-13 1.s0E-13 4/1/2002 2.20E-16 9.00E-14 2.2sE-14 3.38E-16 2.00E-14 s.00E-1s 1.26E-16 9.00E-13 2.2sE-13 7.48E-1s 6.00E-13 l.sOE-13 7/1/2002 1.97E-16 9.00E-14 2.2sE-14 4.lOE-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 7.40E-1s 6.00E-13 l.sOE-13 9/30/2002 2.30E-16 9.00E-14 2.2sE-14 2.42E-16 2.00E-14 s.00E-1s 1.s6E-16 9.00E-13 2.2sE-13 4.21E-1s 6.00E-13 l.sOE-13 12/30/2002 1.00E-16 9.00E-14 2.2sE-14 1.92E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 9.42E-1s 6.00E-13 l.sOE-13 3/31/2003 2.s0E-16 9.00E-14 2.2sE-14 1.69E-16 2.00E-14 s.00E-1s 1.29E-16 9.00E-13 2.2sE-13 4.ssE-1s 6.00E-13 l.sOE-13 6/30/2003 1.00E-16 9.00E-14 2.2sE-14 2.87E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 4.20E-1s 6.00E-13 1.s0E-13 9/29/2003 1.00E-16 9.00E-14 2.2sE-14 8.s3E-16 2.00E-14 s.00E-1s 3.32E-16 9.00E-13 2.2sE-13 8.69E-1s 6.00E-13 1.s0E-13 12/29/2003 1.02E-16 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.49E-1s 9.00E-13 2.2sE-13 9.4sE-1s 6.00E-13 l.sOE-13 3/29/2004 1.00E-16 9.00E-14 2.2sE-14 1.26E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 2.00E-1s 6.00E-13 l.sOE-13 6/27/2004 1.00E-16 9.00E-14 2.2sE-14 2.s3E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 3.23E-1s 6.00E-13 l.sOE-13 9/27/2004 1.00E-16 9.00E-14 2.2sE-14 1.1sE-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 9.68E-1s 6.00E-13 l.sOE-13 12/27/2004 1.00E-16 9.00E-14 2.2sE-14 2.30E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 l.37E-14 6.00E-13 l.sOE-13 3/28/2005 1.00E-16 9.00E-14 2.2sE-14 2.66E-16 2.00E-14 s.00E-1s 3.1sE-16 9.00E-13 2.2sE-13 9.22E-1S 6.00E-13 l.sOE-13 6/29/2005 1.47E-16 9.00E-14 2.2sE-14 1.4sE-1s 2.00E-14 s.00E-1s 1.42E-16 9.00E-13 2.2sE-13 9.34E-1s 6.00E-13 l.sOE-13 9/26/2005 2.01E-16 9.00E-14 2.2sE-14 2.06E-16 2.00E-14 s.00E-1s 4.80E-16 9.00E-13 2.2sE-13 2.12E-14 6.00E-13 l.sOE-13 1/3/2006 4.s4E-16 9.00E-14 2.2sE-14 1.24E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 3.60E-14 6.00E-13 l.sOE-13 4/3/2006 1.99E-16 9.00E-14 2.2sE-14 1.32E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 8.36E-1s 6.00E-13 l.sOE-13 7/3/2006 2.76E-16 9.00E-14 2.2sE-14 2.63E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.03E-14 6.00E-13 l.sOE-13 10/2/2006 4.97E-16 9.00E-14 2.2sE-14 2.37E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.60E-14 6.00E-13 l.sOE-13 1/1/2007 6.46E-16 9.00E-14 2.2sE-14 2.8lE-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 2.10E-14 6.00E-13 l.sOE-13 4/2/2007 7.08E-16 9.00E-14 2.2sE-14 3.20E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 1.s4E-14 6.00E-13 1.s0E-13 7/2/2007 9.41E-16 9.00E-14 2.2sE-14 1.46E-16 2.00E-14 s.00E-1s 1.99E-16 9.00E-13 2.2sE-13 2.s6E-14 6.00E-13 l.sOE-13 9/30/2007 3.30E-16 9.00E-14 2.2sE-14 s.sOE-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 7.s7E-1s 6.00E-13 l.sOE-13 12/31/2007 1.42 E-1s 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 9.93E-1s 6.00E-13 l.sOE-13 3/31/2008 1.2sE-16 9.00E-14 2.2sE-14 7.72E-16 2.00E-14 s.00E-1s 1.00E-16 9.00E-13 2.2sE-13 4.09E-1s 6.00E-13 l.sOE-13 6/30/2008 1.28E-1s 9.00E-14 2.2sE-14 1.00E-16 2.00E-14 s.00E-1S 3.61E-16 9.00E-13 2.2sE-13 1.18E-14 6.00E-13 1.s0E-13 9/30/2008 2.72E-1s 9.00E-14 2.2sE-14 1.27E-1s 2.00E-14 s.00E-1s 7.66E-16 9.00E-13 2.2sE-13 1.10E-14 6.00E-13 1.s0E-13 12/31/2008 2.88E-1s 9.00E-14 2.2sE-14 1.10E-1s 2.00E-14 s.00E-1s 6.s6E-16 9.00E-13 2.2sE-13 l.38E-14 6.00E-13 l.sOE-13 3/15/2009 l.s6E-1s 9.00E-14 2.2sE-14 4.s7E-16 2.00E-14 s.00E-1s 2.99E-16 9.00E-13 2.2sE-13 4.97E-1s 6.00E-13 l.sOE-13 6/15/2009 s.67E-17 9.00E-14 2.2sE-14 2.17E-16 2.00E-14 s.00E-1s l.s1E-16 9.00E-13 2.2sE-13 4.47E-1s 6.00E-13 l.sOE-13 9/15/2009 4.0sE-1s 9.00E-14 2.2sE-14 1.4sE-1s 2.00E-14 s.00E-1s 2.s2E-16 9.00E-13 2.2sE-13 1.24E-14 6.00E-13 l.sOE-13 12/15/2009 6.s0E-1s 9.00E-14 2.2sE-14 3.48E-16 2.00E-14 s.00E-1s l.33E-16 9.00E-13 2.2sE-13 7.60E-1s 6.00E-13 l.sOE-13 ------ Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-4U Effluent Concentration Limit = 2E-14 uCi/ml BHV-4T Effluent Concentration Limit = 9E-13 uCi/ml BHV-4R Effluent Concentration Limit = 6E-13 uCi/ml BHV-4PB ALARA Goal = 2.2SE-14 uCi/ml ALARA Goal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 3/31/2010 6.01E-1S 9.00E-14 2.2SE-14 1.26E-16 2.00E-14 S.00E-1S l.34E-16 9.00E-13 2.2SE-13 1.19E-14 6.00E-13 1.S0E-13 6/30/2010 2.33E-1S 9.00E-14 2.2SE-14 7.29E-16 2.00E-14 S.00E-1S 2.66E-16 9.00E-13 2.2SE-13 3.27E-1S 6.00E-13 1.S0E-13 9/30/2010 4.77E-1S 9.00E-14 2.2SE-14 1.80E-1S 2.00E-14 S.00E-1S 8.23E-16 9.00E-13 2.2SE-13 S.l1E-1S 6.00E-13 1.S0E-13 12/31/2010 3.93E-1S 9.00E-14 2.2SE-14 3.90E-16 2.00E-14 S.00E-1S 2.S6E-16 9.00E-13 2.2SE-13 1.13E-14 6.00E-13 1.S0E-13 4/4/2011 1.29E-1S 9.00E-14 2.2SE-14 1.40E-16 2.00E-14 S.00E-1S 1.S8E-16 9.00E-13 2.2SE-13 l.1IE-14 6.00E-13 1.S0E-13 7/4/2011 3.30E-1S 9.00E-14 2.2SE-14 S.44E-16 2.00E-14 S.00E-1S 4.18E-16 9.00E-13 2.2SE-13 8.26E-1S 6.00E-13 1.S0E-13 10/3/2011 1.32E-1S 9.00E-14 2.2SE-14 7.89E-16 2.00E-14 S.00E-1S 1.28E-16 9.00E-13 2.2SE-13 1.18E-14 6.00E-13 1.S0E-13 1/3/2012 1.04E-1S 9.00E-14 2.2SE-14 3.2SE-16 2.00E-14 S.00E-1S 2.28E-16 9.00E-13 2.2SE-13 1.14E-14 6.00E-13 1.S0E-13 4/3/2012 2.S1E-1S 9.00E-14 2.2SE-14 S.02E-16 2.00E-14 S.00E-1S 2.27E-16 9.00E-13 2.2SE-13 1.03E-14 6.00E-13 1.S0E-13 7/2/2012 2.62E-1S 9.00E-14 2.2SE-14 1.23E-1S 2.00E-14 S.00E-1S 2.97E-16 9.00E-13 2.2SE-13 9.27E-1S 6.00E-13 1.S0E-13 -E ::::: U :1 - N T""" I W 0 ~ T""" C") T""" I W 0 ~ T""" ~i I ..... ! ...... iIi I I ~ L() <0 T""" T""" T""" I I I W W W 0 0 0 ~ ~ ~ T""" T""" (ele~s 001) ~ ~-des o~-des 60-deS go-des LO-deS 90-deS so-des vO-deS 0 T""" £O-deS N I "'0 ro lO-deS Q) .....J ~o-des t OO-deS <0 N N 66-deS I E .2 g6-deS "'0 ro 0::: L6-deS t 96-deS 0 S6-deS C") N I v6-deS E :::J ·c 0 £6-deS ..c I- l6-deS t ~6-des ro ~ ..... ,.. 06-deS :::J ro z 6g-deS E .2 gg-deS c ro ~ :::> Lg-deS t 9g-deS Sg-deS vg-des £g-deS 19-deS ~g-des I"--cx::> T""" T""" I I W W 0 0 ~ ~ T""" T""" 1.00E-11 Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCilml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml BHV-4 Uranium-Natural Concentrations (uCi/ml) 1.00E-12 tg~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~@ 1.00E-13 ~.-.. -............................ -.--... ---.----.. --.---.--.. --.-----.. -.---.--.--.. -..... --.--.--... -.--.-----.-.--.-.-.--.-... -. t m ~ ------==::==::::=====:~==:~~~~~.=:=:~:=---- co ___ ......................... _._ ~ .00E-14 0) ~ ----- 1 .00 E -1 6 __________________ _ ______ . __________________ .=--==.=--==.=--==.=--== ________ _ ~ ....................... -.....••.....•. _-_ ...•.... _._--. -...... _._-....... . ~. -- 1.00E-17 T""" N C"') ~ L() co I"-ex> 0') 0 T""" N C"') ~ L() co I"-ex> 0') 0 T""" N C"') ~ L() co I"-ex> 0') 0 T""" ex> ex> ex> ex> ex> ex> ex> ex> ex> 0') 0') 0') 0') 0') 0') 0') 0') 0') 0') 0 0 0 0 0 0 0 0 0 0 T""" T""" I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) en en en en en en en en en en en en en en en en en en en en en en en en en en en en en en en 1.00E-11 Effluent Concentration Limit = 2E-14 uCi/ml ALARA Goal = 5E-13 uCi/ml Pre 1994 MPC Limit = 8E-14uCi/ml BHV-4 Thorium-230 Concentrations (uCi/ml) 1.00E-12 1===============================================================================1 1.00E-13 ~ .. _ _ _ _ _ ] =.:=?: ..... ==: .. :: ... :=:=:=:: .. := .......... ::: ... :: .. :::: ... =:: .. : .. =:: ..... ::::=:: .. :: .. :::=: ..... =:: ........................................................................................................ ···::f=:::~· :.:::::::.::::::=: .. ~:~=:=::::::.::::~::~: .. ::::=::::=:::::=::~:===::=:=:=~=:=:::::::=: ... ==::===::::=:=:=::::=:= -::=::==:::==::::=:::==:::::=::: .. ==::::::==:==::==::= ... ::=::: ..... ::=:==:= :::::::==:==:~=:::::::= • ---I ............................... -.................. -...... , ......................................... -............................ { .................. -............. -............................................................... ···················1 ············ ! -00 E -141 ... ~::,":::cc,,::=,::='cc==,::::: •• ::::IlJl:-.::....::=_::..::_:_:_.=:::. :::::::::~.:::,,:c:::::_::=: ____ ----co---------------------------------::::':=:::':cc=':c:=:,,'c",=::::'::::: o ::::. 1_00E-15 ------------------------------------------=--==------~~-~ ................................................. __ . __ .. _ .•.. I·· .. ······.. .-.. -.---.. ----.. - 1.00E-16 -----_._----------------------_ .. _----------------------------------------==============~-------------------~=== .............................. -............ :::=:::=:::= ~-~~~---~~===~ 1.00E-17 ~ N C"'.) ~ LO co "-ex:.> C) 0 ~ N C"'.) ~ LO co "-ex:.> C) 0 ~ N C"'.) ~ LO co "-ex:.> C) 0 ex:.> ex:.> ex:.> ex:.> ex:.> ex:.> ex:.> ex:.> ex:.> C) C) C) C) C) C) C) C) C) C) 0 0 0 0 0 0 0 0 0 0 ~ ~ I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) en en en en en en en en en en en en en en en en en en en en en en en en en en en en en en en 1.00E-11 Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml BHV-4 Radium-226 Concentrations (uCi/ml) 1.00E-12 I .............. u ••• u .......................... ~ I .. -------_ .. ----_ .. ----_ ...... -_ .. ------_._ .. --._---_... .. ... _-..... . ---__ -= -_-_ ::-=_-=-_ =_ -=_-___ -u-:.._-= -_ -= -= ____ -= _______ =-= __ -__ -= -=_-:.. _ _ _ ____ -= _________ = __ .-_=-= _ _ m ;-_ -_ -:.. _. _ _ -_ _ ________________ ...::...:: ________________________________ ~ _______ ~ __ ~ ____ --_. ___ -_~ ~ ______ ~ ____ ~ \ ~ 1.00E-13 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ ...l... 00 E -1 4 .---.. -.. --.-.. ---------.-------::_::::::::::::::::::::~:::::::::::::::::::::::~_:::~_:::.:::::::::::::~::::::_::::::::::::::::::::::::::::-::::::::::::=:::::::::::::::::.:::::::-:::::::::::~_::::--.--.--.--.------.-.. -::::::::::::::_.::-.. -.-----------.-.. -... --.-... ---.. ---...... --------.-:::: .................................. ~ ......................... -..... -........................................... -...... -... -..... - Q) ------------------------------------------------------====---==::.::.===========---============================-===:===:====:::===:::::::::::::::=====:===::::..--======--ro ......... -... --...... -..... -.-........... -... -... -... -..... -...... -..... -.-... -... -... -... --.-... -... --.-... -u CI) 0> .................. -...... -... -...... -.---.-... -..... -.--.. J o .....J '"f. 00 E -1 5 ........ ::~~~_=::~~:::~~ .... _. 1.00E-16 .... _---_._------_. __ ... __ ._-_ ...... _--_ ... _ .. _-_ ... _ .. --_._-----_._---_ ..... _--_ ....... _. __ ._ .. _--_._-_._ .. __ ._---_ ..... _---_._------------------_._ .. _---------------------_ .. --------_._-_._-------------.-.--_.-.. _-.-.......... -.. __ ... _.-._ .•. _ ... _--._ ... __ ._ ... _ ... _ ... _ .. _- .... _--_. __ ._--------_ ... _ ... _-_._--_ ... __ ._---_._. __ .. _-------------- 1.00E-17 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-18 T""" C\I ("I") ..".. L{) c.o "-co 0"> 0 T""" C\I ("I") ..".. L{) c.o "-co 0"> 0 T""" C\I ("I") ..".. L{) c.o "-co 0"> 0 T""" co co co co co co co co co 0"> 0"> 0"> 0"> 0"> 0"> 0"> 0"> 0"> 0"> 0 0 0 0 0 0 0 0 0 0 T""" T""" I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) CI) 1.00E-11 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1 E-12 uCi/ml BHV-4 Lead-210 Concentrations (uCi/ml) I , I 1.00E-13 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ (j) m u CIl.OOE-14 C) o ::::.. • 1 .OOE-15 g-===---~-----1=---------------------------------.--·!l-----.. ·· .. -· ...... · .. ··· .. · .... -.... · ...... ··· .... · ........ · .... ··· ................................................................................................................................. -............... . ........ -................ ~...... . ............................................. : ... ~~ ...... ~·· .. ···1 1.00E-16 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-17 ~ N ("I) ~ LO co I"-co 0) 0 ~ N ("I) ~ LO co I"-co 0) 0 ~ N ("I) ~ LO co I"-co 0) 0 co co co co co co co co co 0) 0) 0) 0) 0) 0) 0) 0) 0) 0) 0 0 0 0 0 0 0 0 0 0 ~ ~ I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. c.. Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) Q.) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) TAB 5 BHV-5 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit = 6E-13 uCi/ml BHV-SPB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 2.44E-1S S.00E-12 l.2sE-12 1.s3E-1S 8.00E-14 2.00E-14 7.s4E-16 2.00E-12 s.OOE-13 1.69E-14 4.00E-12 1.00E-12 12/14/1981 4.84E-1s S.00E-12 l.2sE-12 2.78E-1s 8.00E-14 2.00E-14 1.84E-1S 2.00E-12 S.OOE-13 1.s3E-14 4.00E-12 1.00E-12 3/29/1982 1.04E-1S S.00E-12 1.2sE-12 2.62E-1S 8.00E-14 2.00E-14 1.11E-1s 2.00E-12 S.OOE-13 2.98E-14 4.00E-12 1.00E-12 6/30/1982 3.6lE-1S S.00E-12 1.2SE-12 7.61E-1S 8.00E-14 2.00E-14 1.39E-1s 2.00E-12 S.OOE-13 1.80E-1S 4.00E-12 1.00E-12 9/27/1982 1.71E-14 s.00E-12 l.2sE-12 9.46E-1S 8.00E-14 2.00E-14 3.80E-1S 2.00E-12 s.OOE-13 2.3sE-14 4.00E-12 1.00E-12 1/3/1983 1.90E-14 s.00E-12 1.2SE-12 S.77E-1s 8.00E-14 2.00E-14 9.34E-17 2.00E-12 S.OOE-13 4.32E-14 4.00E-12 1.00E-12 4/4/1983 S.00E-12 l.2sE-12 2.33E-1S 8.00E-14 2.00E-14 s.93E-16 2.00E-12 S.OOE-13 3.0lE-14 4.00E-12 1.00E-12 6/30/1983 7.62E-16 s.00E-12 l.2sE-12 3.2sE-1s 8.00E-14 2.00E-14 6.28E-1s 2.00E-12 s.OOE-13 2.69E-14 4.00E-12 1.00E-12 10/3/1983 4.86E-16 s.00E-12 l.2SE-12 1.10E-1s 8.00E-14 2.00E-14 3.63E-16 2.00E-12 S.OOE-13 2.08E-14 4.00E-12 1.00E-12 1/3/1984 6.96E-1s s.00E-12 l.2SE-12 9.69E-16 8.00E-14 2.00E-14 9.60E-16 2.00E-12 S.OOE-13 1.83E-14 4.00E-12 1.00E-12 4/2/1984 1.64E-1s S.00E-12 1.2SE-12 1.34E-1s 8.00E-14 2.00E-14 3.88E-1s 2.00E-12 S.OOE-13 4.67E-14 4.00E-12 1.00E-12 7/2/1984 1.12E-1s s.00E-12 1.2SE-12 1.92E-1s 8.00E-14 2.00E-14 3.31E-1S 2.00E-12 S.OOE-13 2.21E-14 4.00E-12 1.00E-12 10/1/1984 1.1lE-1s S.00E-12 1.2SE-12 3.13E-16 8.00E-14 2.00E-14 4.21E-16 2.00E-12 S.OOE-13 1.s7E-14 4.00E-12 1.00E-12 1/2/1985 7.32E-16 S.00E-12 1.2sE-12 6.71E-16 8.00E-14 2.00E-14 4.94E-16 2.00E-12 s.OOE-13 2.42E-14 4.00E-12 1.00E-12 4/1/1985 2.36E-16 S.00E-12 l.2sE-12 S.43E-16 8.00E-14 2.00E-14 2.71E-16 2.00E-12 S.OOE-13 l.2sE-14 4.00E-12 1.00E-12 7/1/1985 7.s8E-16 s.OOE-12 l.2SE-12 4.00E-16 8.00E-14 2.00E-14 6.90E-16 2.00E-12 S.OOE-13 2.1SE-14 4.00E-12 1.00E-12 9/30/1985 7.47E-1S s.00E-12 l.2SE-12 1.16E-1S 8.00E-14 2.00E-14 2.19E-1S 2.00E-12 S.OOE-13 9.20E-1s 4.00E-12 1.00E-12 1/2/1986 1.7sE-14 S.00E-12 1.2SE-12 7.24E-1S 8.00E-14 2.00E-14 3.83E-1S 2.00E-12 s.OOE-13 1.13E-16 4.00E-12 1.00E-12 4/1/1986 2.99E-14 S.00E-12 1.2SE-12 7.64E-1S 8.00E-14 2.00E-14 1.S1E-14 2.00E-12 S.OOE-13 2.22E-14 4.00E-12 1.00E-12 6/30/1986 2.23E-14 S.00E-12 l.2sE-12 S.19E-1s 8.00E-14 2.00E-14 1.0sE-14 2.00E-12 s.OOE-13 2.16E-14 4.00E-12 1.00E-12 10/27/1986 2.33E-14 s.00E-12 l.2sE-12 7.78E-1s 8.00E-14 2.00E-14 1.60E-14 2.00E-12 s.OOE-13 2.02E-14 4.00E-12 1.00E-12 12/15/1986 3.40E-14 S.00E-12 l.2SE-12 S.3SE-1S 8.00E-14 2.00E-14 1.47E-14 2.00E-12 S.OOE-13 2.82E-14 4.00E-12 1.00E-12 3/16/1987 2.06E-14 S.00E-12 1.2SE-12 4.S0E-1S 8.00E-14 2.00E-14 6.74E-1s 2.00E-12 S.OOE-13 7.29E-14 4.00E-12 1.00E-12 5/11/1987 2.S0E-14 S.00E-12 1.2sE-12 8.S4E-1S 8.00E-14 2.00E-14 8.1SE-1S 2.00E-12 S.OOE-13 3.28E-14 4.00E-12 1.00E-12 9/9/1987 2.6sE-14 s.OOE-12 l.2sE-12 6.62E-1S 8.00E-14 2.00E-14 9.34E-1s 2.00E-12 s.OOE-13 2.77E-14 4.00E-12 1.00E-12 11/2/1987 1.80E-14 S.00E-12 l.2SE-12 7.09E-1s 8.00E-14 2.00E-14 7.20E-1S 2.00E-12 S.OOE-13 1.77E-14 4.00E-12 1.00E-12 2/16/1988 1.01E-14 s.00E-12 1.2SE-12 2.98E-1s 8.00E-14 2.00E-14 3.93E-1s 2.00E-12 s.OOE-13 3.36E-14 4.00E-12 1.00E-12 5/18/1988 1.78E-14 s.00E-12 1.2SE-12 8.14E-1S 8.00E-14 2.00E-14 7.43E-1s 2.00E-12 s.OOE-13 2.12E-14 4.00E-12 1.00E-12 8/15/1988 1.79E-14 S.00E-12 1.2sE-12 1.49E-14 8.00E-14 2.00E-14 S.34E-1s 2.00E-12 S.OOE-13 2.4SE-14 4.00E-12 1.00E-12 11/14/1988 4.46E-14 S.00E-12 1.2sE-12 1.39E-14 8.00E-14 2.00E-14 1.17E-14 2.00E-12 s.OOE-13 3.43E-14 4.00E-12 1.00E-12 2/13/1989 1.67E-14 S.00E-12 l.2SE-12 s.s4E-1s 8.00E-14 2.00E-14 7.20E-1S 2.00E-12 s.OOE-13 S.02E-14 4.00E-12 1.00E-12 5/15/1989 2.03E-14 s.00E-12 1.2SE-12 7.0SE-1s 8.00E-14 2.00E-14 9.S6E-16 2.00E-12 s.OOE-13 1.43E-14 4.00E-12 1.00E-12 8/14/1989 2.81E-1s s.00E-12 1.2SE-12 3.78E-1S 8.00E-14 2.00E-14 9.26E-1S 2.00E-12 s.OOE-13 1.S0E-14 4.00E-12 1.00E-12 11/13/1989 S.38E-14 S.00E-12 1.2sE-12 8.01E-1s 8.00E-14 2.00E-14 1.8lE-14 2.00E-12 s.OOE-13 4.09E-14 4.00E-12 1.00E-12 2/12/1990 4.48E-14 S.00E-12 1.2sE-12 1.48E-14 8.00E-14 2.00E-14 l.28E-14 2.00E-12 s.OOE-13 3.88E-14 4.00E-12 1.00E-12 5/14/1990 2.18E-14 S.00E-12 l.2SE-12 1.70E-14 8.00E-14 2.00E-14 1.59E-14 2.00E-12 S.OOE-13 3.49E-14 4.00E-12 1.00E-12 8/13/1990 9.S3E-1S s.00E-12 1.2sE-12 1.70E-14 8.00E-14 2.00E-14 3.27E-1S 2.00E-12 S.OOE-13 1.27E-14 4.00E-12 1.00E-12 11/12/1990 1.11E-14 s.00E-12 1.2SE-12 S.27E-1S 8.00E-14 2.00E-14 s.38E-1S 2.00E-12 S.OOE-13 1.S6E-14 4.00E-12 1.00E-12 2/11/1991 6.3SE-16 S.00E-12 1.2SE-12 3.13E-16 8.00E-14 2.00E-14 2.3lE-16 2.00E-12 S.OOE-13 3.89E-14 4.00E-12 1.00E-12 5/13/1991 l.22E-1s s.00E-12 l.2sE-12 6.14E-1S 8.00E-14 2.00E-14 4.4lE-1s 2.00E-12 s.OOE-13 2.s0E-14 4.00E-12 1.00E-12 8/12/1991 7.84E-16 s.00E-12 1.2sE-12 1.43E-1S 8.00E-14 2.00E-14 4.47E-16 2.00E-12 S.OOE-13 1.84E-14 4.00E-12 1.00E-12 11/11/1991 S.37E-16 S.00E-12 1.2SE-12 4.20E-16 8.00E-14 2.00E-14 1.37E-16 2.00E-12 S.OOE-13 1.27E-14 4.00E-12 1.00E-12 2/10/1992 3.S4E-16 S.00E-12 1.2SE-12 1.18E-16 8.00E-14 2.00E-14 4.08E-17 2.00E-12 S.OOE-13 3.69E-14 4.00E-12 1.00E-12 5/11/1992 4.71E-16 S.00E-12 1.2SE-12 9.S8E-16 8.00E-14 2.00E-14 8.31E-17 2.00E-12 S.OOE-13 1.43E-14 4.00E-12 1.00E-12 8/10/1992 S.32E-1s s.00E-12 1.2sE-12 3.36E-16 8.00E-14 2.00E-14 1.6sE-16 2.00E-12 s.OOE-13 1.S9E-14 4.00E-12 1.00E-12 11/9/1992 3.66E-16 S.00E-12 1.2SE-12 2.2SE-16 8.00E-14 2.00E-14 1.08E-16 2.00E-12 s.OOE-13 2.24E-14 4.00E-12 1.00E-12 2/9/1993 2.0sE-16 s.00E-12 l.2SE-12 9.14E-17 8.00E-14 2.00E-14 6.3lE-17 2.00E-12 S.OOE-13 3.41E-14 4.00E-12 1.00E-12 5/10/1993 4.80E-16 s.00E-12 1.2SE-12 8.2SE-16 8.00E-14 2.00E-14 1.26E-1s 2.00E-12 S.OOE-13 1.83E-14 4.00E-12 1.00E-12 8/10/1993 8.30E-16 S.00E-12 1.2SE-12 1.90E-16 8.00E-14 2.00E-14 2.lOE-16 2.00E-12 S.OOE-13 1.70E-14 4.00E-12 1.00E-12 11/8/1993 2.70E-16 S.00E-12 l.2SE-12 8.00E-17 8.00E-14 2.00E-14 7.00E-17 2.00E-12 S.OOE-13 2.34E-14 4.00E-12 1.00E-12 2/7/1994 3.18E-16 S.00E-12 1.2sE-12 1.00E-16 8.00E-14 2.00E-14 s.18E-16 2.00E-12 s.OOE-13 3.64E-14 4.00E-12 1.00E-12 5/9/1994 1.80E-1s s.OOE-12 1.2SE-12 9.78E-16 8.00E-14 2.00E-14 1.10E-1S 2.00E-12 s.OOE-13 8.30E-1s 4.00E-12 1.00E-12 8/9/1994 2.67E-1s S.OOE-12 1.2sE-12 1.11E-1s 8.00E-14 2.00E-14 4.9sE-16 2.00E-12 s.OOE-13 1.00E-16 4.00E-12 1.00E-12 11/7/1994 9.21E-17 S.00E-12 1.2SE-12 1.S9E-1S 8.00E-14 2.00E-14 1.66E-1S 2.00E-12 S.OOE-13 1.00E-16 4.00E-12 1.00E-12 2/7/1995 1.s1E-1S 9.00E-14 2.2sE-14 9.S0E-16 2.00E-14 S.00E-1s 9.70E-17 9.00E-13 2.2sE-13 9.3sE-1s 6.00E-13 1.s0E-13 5/9/1995 2.21E-16 9.00E-14 2.2SE-14 8.S6E-16 2.00E-14 S.00E-1S 3.06E-1S 9.00E-13 2.2sE-13 4.34E-1s 6.00E-13 1.s0E-13 8/9/1995 1.66E-16 9.00E-14 2.2SE-14 1.67E-1s 2.00E-14 s.00E-1S 3.90E-1S 9.00E-13 2.2SE-13 S.60E-1S 6.00E-13 1.S0E-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit = 6E-13 uCi/ml BHV-SPB ALARA Goal = 2.2SE-14 uCi/ml ALARA Goal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARA Goal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 11/11/1995 2.04E-14 9.00E-14 2.2sE-14 6.70E-1s 2.00E-14 s.00E-1s 7.6sE-1s 9.00E-13 2.2sE-13 4.47E-1s 6.00E-13 l.sOE-13 2/5/1996 4.s0E-14 9.00E-14 2.2sE-14 3.s8E-14 2.00E-14 s.00E-1s 2.39E-14 9.00E-13 2.2sE-13 7.30E-1s 6.00E-13 l.sOE-13 5/6/1996 l.76E-1s 9.00E-14 2.2sE-14 3.s7E-1s 2.00E-14 s.00E-1s 9.ssE-16 9.00E-13 2.2sE-13 7.s4E-1s 6.00E-13 l.sOE-13 8/5/1996 2.37E-1s 9.00E-14 2.2sE-14 8.18E-1s 2.00E-14 s.00E-1s 7.46E-16 9.00E-13 2.2sE-13 s.7sE-1s 6.00E-13 l.sOE-13 11/6/1996 3.s3E-1s 9.00E-14 2.2sE-14 s.31E-1s 2.00E-14 s.00E-1s 9.39E-16 9.00E-13 2.2sE-13 l.21E-14 6.00E-13 l.SOE-13 2/6/1997 l.84E-16 9.00E-14 2.2sE-14 2.01E-16 2.00E-14 s.00E-1s l.87E-16 9.00E-13 2.2sE-13 6.14E-1s 6.00E-13 l.sOE-13 5/5/1997 s.7sE-16 9.00E-14 2.2sE-14 7.24E-16 2.00E-14 s.00E-1s 6.07E-16 9.00E-13 2.2sE-13 4.7sE-1s 6.00E-13 l.sOE-13 8/11/1997 1.21E-1s 9.00E-14 2.2sE-14 7.39E-16 2.00E-14 s.00E-1S s.OsE-16 9.00E-13 2.2sE-13 4.92E-1s 6.00E-13 1.s0E-13 1/5/1998 9.89E-16 9.00E-14 2.2sE-14 l.92E-1s 2.00E-14 s.00E-1s 6.21E-16 9.00E-13 2.2sE-13 4.68E-1s 6.00E-13 1.s0E-13 4/28/1998 2.84E-1s 9.00E-14 2.2sE-14 2.38E-1s 2.00E-14 s.00E-1S l.72E-1s 9.00E-13 2.2sE-13 7.3sE-1s 6.00E-13 l.sOE-13 7/31/1998 7.49E-16 9.00E-14 2.2SE-14 1.49E-1s 2.00E-14 s.00E-1s 8.34E-16 9.00E-13 2.2sE-13 7.0lE-1s 6.00E-13 l.sOE-13 9/28/1998 l.07E-1s 9.00E-14 2.2sE-14 9.20E-16 2.00E-14 s.00E-1s 6.32E-16 9.00E-13 2.2sE-13 3.9sE-1s 6.00E-13 l.sOE-13 12/28/1998 8.slE-1s 9.00E-14 2.2sE-14 4.s8E-1S 2.00E-14 s.00E-1s 4.s8E-1s 9.00E-13 2.2SE-13 l.43E-14 6.00E-13 l.sOE-13 3/29/1999 3.7sE-1s 9.00E-14 2.2sE-14 2.4sE-1S 2.00E-14 s.00E-1s 2.39E-1s 9.00E-13 2.2SE-13 8.46E-1s 6.00E-13 l.sOE-13 7/3/1999 l.s3E-1s 9.00E-14 2.2sE-14 8.6sE-16 2.00E-14 s.00E-1s 6.s2E-16 9.00E-13 2.2sE-13 7.20E-1S 6.00E-13 l.sOE-13 9/27/1999 s.83E-1S 9.00E-14 2.2sE-14 3.S2E-1S 2.00E-14 s.00E-1s 2.5sE-1s 9.00E-13 2.2sE-13 8.22E-1S 6.00E-13 1.s0E-13 12/28/1999 9.48E-1s 9.00E-14 2.2sE-14 6.20E-1s 2.00E-14 s.00E-1s 3.96E-1s 9.00E-13 2.2sE-13 7.s6E-1s 6.00E-13 1.s0E-13 3/27/2000 2.06E-1S 9.00E-14 2.2sE-14 1.27E-1s 2.00E-14 s.00E-1s l.09E-1s 9.00E-13 2.2sE-13 7.72E-1s 6.00E-13 l.sOE-13 6/26/2000 l.sOE-1s 9.00E-14 2.2sE-14 1.24E-1s 2.00E-14 s.00E-1s l.01E-1s 9.00E-13 2.2sE-13 4.36E-1s 6.00E-13 l.sOE-13 9/26/2000 l.04E-1s 9.00E-14 2.2sE-14 s.4SE-16 2.00E-14 s.00E-1s 6.01E-16 9.00E-13 2.2sE-13 7.67E-1s 6.00E-13 l.sOE-13 12/26/2000 l.48E-1s 9.00E-14 2.2sE-14 7.s6E-16 2.00E-14 s.00E-1s 6.84E-16 9.00E-13 2.2sE-13 7.00E-1s 6.00E-13 l.sOE-13 3/26/2001 4.27E-16 9.00E-14 2.2sE-14 2.19E-16 2.00E-14 s.00E-1s l.89E-16 9.00E-13 2.2sE-13 6.13E-1S 6.00E-13 l.SOE-13 7/2/2001 4.s2E-16 9.00E-14 2.2sE-14 4.02E-16 2.00E-14 S.00E-1s l.00E-16 9.00E-13 2.2sE-13 7.48E-1s 6.00E-13 1.s0E-13 9/24/2001 4.6sE-16 9.00E-14 2.2sE-14 2.06E-16 2.00E-14 s.00E-1s 2.02E-16 9.00E-13 2.2sE-13 6.98E-1s 6.00E-13 1.s0E-13 12/31/2001 7.40E-16 9.00E-14 2.2sE-14 3.S1E-16 2.00E-14 s.00E-1s 3.64E-16 9.00E-13 2.2sE-13 4.72E-1s 6.00E-13 1.s0E-13 4/1/2002 1.26E-1s 9.00E-14 2.2sE-14 7.s3E-16 2.00E-14 s.00E-1s 7.19E-16 9.00E-13 2.2sE-13 9.6sE-1s 6.00E-13 l.sOE-13 7/1/2002 l.02E-1s 9.00E-14 2.2sE-14 l.03E-1s 2.00E-14 s.00E-1S 3.39E-16 9.00E-13 2.2sE-13 7.20E-1s 6.00E-13 l.sOE-13 9/30/2002 s.82E-16 9.00E-14 2.2sE-14 9.28E-16 2.00E-14 s.00E-1s 3.14E-16 9.00E-13 2.2sE-13 4.48E-1s 6.00E-13 l.sOE-13 12/30/2002 l.00E-16 9.00E-14 2.2sE-14 7.67E-16 2.00E-14 s.00E-1s 3.48E-16 9.00E-13 2.2sE-13 9.s6E-1s 6.00E-13 l.sOE-13 3/31/2003 l.13E-1S 9.00E-14 2.2sE-14 7.41E-16 2.00E-14 s.00E-1s 4.41E-16 9.00E-13 2.2sE-13 6.68E-1s 6.00E-13 l.sOE-13 6/30/2003 4.3SE-16 9.00E-14 2.2sE-14 s.08E-16 2.00E-14 s.00E-1s 2.s1E-16 9.00E-13 2.2sE-13 l.34E-1s 6.00E-13 l.sOE-13 9/29/2003 l.slE-16 9.00E-14 2.2sE-14 1.02E-16 2.00E-14 s.00E-1s l.00E-16 9.00E-13 2.2sE-13 7.28E-1s 6.00E-13 l.sOE-13 12/29/2003 l.s2E-16 9.00E-14 2.2sE-14 1.s4E-16 2.00E-14 s.00E-1s l.slE-16 9.00E-13 2.2sE-13 7.02E-1s 6.00E-13 1.s0E-13 3/29/2004 l.00E-16 9.00E-14 2.2SE-14 1.12E-16 2.00E-14 s.00E-1s l.00E-16 9.00E-13 2.2sE-13 8.82E-1s 6.00E-13 l.sOE-13 6/27/2004 l.18E-16 9.00E-14 2.2sE-14 3.11E-16 2.00E-14 s.00E-1s l.2sE-16 9.00E-13 2.2sE-13 2.47E-1s 6.00E-13 l.SOE-13 9/27/2004 l.16E-16 9.00E-14 2.2sE-14 l.72E-16 2.00E-14 s.00E-1S 1.18E-16 9.00E-13 2.2SE-13 1.10E-14 6.00E-13 l.SOE-13 12/27/2004 l.14E-16 9.00E-14 2.2SE-14 l.06E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 l.59E-14 6.00E-13 l.50E-13 3/28/2005 l.00E-16 9.00E-14 2.2SE-14 2.04E-16 2.00E-14 S.00E-1S l.83E-16 9.00E-13 2.2SE-13 8.s7E-1S 6.00E-13 l.SOE-13 6/29/2005 l.83E-16 9.00E-14 2.2sE-14 3.81E-16 2.00E-14 S.00E-1S 3.09E-16 9.00E-13 2.2SE-13 l.06E-14 6.00E-13 l.SOE-13 9/26/2005 2.87E-16 9.00E-14 2.2sE-14 8.21E-16 2.00E-14 S.00E-1S 3.71E-14 9.00E-13 2.2SE-13 6.28E-14 6.00E-13 l.SOE-13 1/3/2006 8.74E-16 9.00E-14 2.2sE-14 3.79E-16 2.00E-14 S.00E-1S l.31E-16 9.00E-13 2.2SE-13 4.32E-14 6.00E-13 l.SOE-13 4/3/2006 S.22E-16 9.00E-14 2.2SE-14 6.66E-16 2.00E-14 S.00E-1S l.l1E-16 9.00E-13 2.2SE-13 9.34E-1S 6.00E-13 l.SOE-13 7/3/2006 3.08E-16 9.00E-14 2.2SE-14 1.10E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 1.2sE-14 6.00E-13 1.S0E-13 10/2/2006 9.14E-16 9.00E-14 2.2SE-14 4.9sE-16 2.00E-14 S.00E-1S l.86E-16 9.00E-13 2.2SE-13 1.67E-14 6.00E-13 l.50E-13 1/1/2007 9.49E-16 9.00E-14 2.2SE-14 6.81E-16 2.00E-14 S.00E-1S 2.02E-16 9.00E-13 2.2sE-13 l.3lE-14 6.00E-13 l.SOE-13 4/2/2007 l.08E-1S 9.00E-14 2.2SE-14 8.22E-16 2.00E-14 S.00E-1S 2.26E-16 9.00E-13 2.2sE-13 l.64E-14 6.00E-13 l.sOE-13 7/2/2007 l.S4E-1S 9.00E-14 2.2SE-14 8.16E-16 2.00E-14 s.00E-1S 4.76E-16 9.00E-13 2.2sE-13 2.12E-14 6.00E-13 l.sOE-13 9/30/2007 4.90E-16 9.00E-14 2.2sE-14 2.37E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 6.6sE-1S 6.00E-13 l.SOE-13 12/31/2007 l.46E-1s 9.00E-14 2.2SE-14 S.67E-16 2.00E-14 S.00E-1S l.00E-16 9.00E-13 2.2SE-13 l.02E-14 6.00E-13 1.S0E-13 3/31/2008 3.16E-16 9.00E-14 2.2sE-14 6.17E-16 2.00E-14 S.00E-1S 3.71E-16 9.00E-13 2.2SE-13 4.82E-1S 6.00E-13 l.SOE-13 6/30/2008 3.13E-1S 9.00E-14 2.2sE-14 l.SsE-1S 2.00E-14 S.00E-1s 9.27E-16 9.00E-13 2.2SE-13 7.40E-1S 6.00E-13 l.SOE-13 9/30/2008 7.08E-1S 9.00E-14 2.2SE-14 3.4lE-1S 2.00E-14 S.00E-1S 2.S2E-1S 9.00E-13 2.2SE-13 1.lSE-14 6.00E-13 l.SOE-13 12/31/2008 7.22E-1S 9.00E-14 2.2SE-14 2.82E-1S 2.00E-14 S.00E-1S 3.03E-1s 9.00E-13 2.2SE-13 l.S9E-14 6.00E-13 l.sOE-13 3/15/2009 4.13E-1S 9.00E-14 2.2SE-14 l.39E-1S 2.00E-14 s.00E-1S l.4lE-1S 9.00E-13 2.2SE-13 4.66E-1S 6.00E-13 l.sOE-13 6/15/2009 2.3lE-16 9.00E-14 2.2SE-14 7.79E-16 2.00E-14 S.00E-1S 6.37E-16 9.00E-13 2.2SE-13 4.18E-1S 6.00E-13 l.SOE-13 9/15/2009 3.lOE-1s 9.00E-14 2.2sE-14 9.20E-16 2.00E-14 S.00E-1S 6.36E-16 9.00E-13 2.2SE-13 l.21E-14 6.00E-13 l.SOE-13 12/15/2009 S.77E-1s 9.00E-14 2.2SE-14 3.13E-16 2.00E-14 S.00E-1S l.92E-16 9.00E-13 2.2SE-13 2.48E-15 6.00E-13 l.SOE-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-SU Effluent Concentration Limit = 2E-14 uCi/ml BHV-ST Effluent Concentration Limit = 9E-13 uCi/ml BHV-SR Effluent Concentration Limit = 6E-13 uCi/ml BHV-SPB · ALARAGoal = 2.2SE-14 uCi/ml ALARA Goal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 3/31/2010 4.7BE-1S 9.00E-14 2.2SE-14 3.73E-16 2.00E-14 S.00E-1S 4.19E-16 9.00E-13 2.2SE-13 1.30E-14 6.00E-13 1.S0E-13 6/30/2010 4.3SE-1S 9.00E-14 2.2SE-14 7.B4E-16 2.00E-14 S.00E-1S 1.0SE-1S 9.00E-13 2.2SE-13 4.40E-1S 6.00E-13 1.S0E-13 9/30/2010 3.S7E-1S 9.00E-14 2.2SE-14 1.14E-1S 2.00E-14 S.00E-1S 7.97E-16 9.00E-13 2.2SE-13 3.7BE-1S 6.00E-13 1.S0E-13 12/31/2010 B.S2E-1S 9.00E-14 2.2SE-14 1.4SE-1S 2.00E-14 S.00E-1S 1.29E-1S 9.00E-13 2.2SE-13 1.33E-14 6.00E-13 1.S0E-13 4/4/2011 3.20E-1S 9.00E-14 2.2SE-14 8.89E-16 2.00E-14 S.00E-1S 1.10E-1S 9.00E-13 2.2SE-13 1.48E-14 6.00E-13 1.S0E-13 7/4/2011 6.98E-1S 9.00E-14 2.2SE-14 2.03E-1S 2.00E-14 S.00E-1S 2.S2E-1S 9.00E-13 2.2SE-13 1.0BE-14 6.00E-13 1.S0E-13 10/3/2011 3.11E-1S 9.00E-14 2.2SE-14 1.14E-1S 2.00E-14 S.00E-1S S.7SE-16 9.00E-13 2.2SE-13 1.41E-14 6.00E-13 1.S0E-13 1/3/2012 4.44E-1S 9.00E-14 2.2SE-14 2.14E-1S 2.00E-14 S.00E-1S 1.S3E-1S 9.00E-13 2.2SE-13 2.0SE-14 6.00E-13 1.S0E-13 4/3/2012 S.S2E-1S 9.00E-14 2.2SE-14 3.24E-1S 2.00E-14 S.00E-1S 1.79E-1S 9.00E-13 2.2SE-13 1.SSE-14 6.00E-13 1.S0E-13 7/2/2012 S.87E-1S 9.00E-14 2.2SE-14 3.06E-1S 2.00E-14 S.00E-1S 1.21E-1S 9.00E-13 2.2SE-13 1.11E-14 6.00E-13 1.S0E-13 -E :::: U :::s - N ('f) T""" T""" I I W W 0 0 ~ ~ I ~ I! Ii ...;:t I.{) T""" T""" I I W W 0 0 ~ ~ T""" (ele~s 001) ~ ~-des o~-des 60-deS go-des LO-deS go-des go-des Po-des 0 T""" £O-deS N I "'C co Go-des Q) .....J ~o-des t OO-deS <0 N N 66-deS I E .~ 96-deS "'C co 0::: L6-deS t 96-deS 0 96-deS ('f) N I P6-deS E :::J ·c 0 £6-deS ..c I- G6-deS t ~6-des co L... 06-deS :::J 10 z 69-deS E .~ gg-deS c co L... => L9-deS t gg-deS gg-deS pg-des £g-deS Gg-deS ~g-des <0 r-.... CX) T""" T""" T""" I I I W W W 0 0 0 ~ ~ ~ T""" T""" 1.00E-11 Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.25E-14 uCi/ml Pre 1994 MPC Limit = 5E-12uCi/ml Pre 1994 ALARA Goal = 1.25E-12 uCilml BHV-5 Uranium-Natural Concentrations (uCilml) 1 . 00E-12 E===================================================I====================================================================~ 1.00E-13 t~~~~~~~~~~~~~~~~~~~~~~~t~~~~~~~==~_=~_==~~~~~=-~=~--~d CD ----=~~:=-:=~=~==t=t~~-~-----------------------------~ ro u ~. OOE -14 __ ~==;.~~~~~~~~~~~=== -~=.~~~=.-~---~-='-~--~-='-~-='-~-~-~--=.:--~~--~--~-='-~---~~--~--~--~-~--=.-~-=.-:=.=.----=.=.--:-=-=.=. :::==.=::=.==.====.==.:=.=.=::==-~=.==.==.===~~=.:=.=.:::=.~~:=.:=.=7't. o _____________________________________________ _ .....J -- 1_00E-15 ==-=--=:=---:1L-_ __I ------------- ------------------------------------------ ~ ... _._--_._--_._-_._------_._-_._------ 1 .00 E -16 ==--=--=-=---==-=-=-==--=-::.::-=--=-=-=--=-====--=-==--=-=--=====.-:.. _________ ==== ___________ ======-_=======:==:===------___ ~==-~-=~~~=:::::=:--__ _ ______ _ --_._-----------_._------------------------------------._-----"------------_ .. _-------------------------------------------------------------- 1.00E-17 ~ C\I C'") ~ L() co I'-cx::> C'> 0 ~ C\I C'") ~ L() co I'-cx::> C'> 0 ~ C\I C'") ~ L() co I'-cx::> C'> 0 cx::> cx::> cx::> cx::> cx::> cx::> cx::> cx::> cx::> C'> C'> C'> C'> C'> C'> C'> C'> C'> C'> 0 0 0 0 0 0 0 0 0 0 ~ ~ I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) 1.00E-11 Effluent Concentration Limit = 2E-14 uCi/ml ALARA Goal = 5E-13 uCi/ml Pre 1994 MPC Limit = 8E-14uCi/ml BHV-5 Thorium-230 Concentrations (uCi/ml) 1.00E-12 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ , !~OE~4 ~~l~~~~~~~~~~~~~~~~~~~~~_~i~~~~~~§~§§~ .. -~~~---l--------------I-: .. . i 1\ ~ ........................................ _ ................. ?j} .................................... _ ....................................................................... . ~____~~~:~~_~:~~§~~~:~~~-:~=-~~~=~=~~~=~~-==E~~~--~~::--: 1 .00 E -1 6 ._ ... __ .. _ ..... _ ...... _ ........... __ .... _ .... _ .............. _ .. _ .. _ ............... _ ... _ ............................. _ ..... _ ..... _ ................... _ ........... _......... . ... _.. . .......................... _ ................. _............................................................ ... ..... ............................................................... .................................... . ...................... _ ............ -._ ...... __ ... _ .................................... -.............. . --------------------_._-----------_._-_._------_ .... _ .... _-.. _--_ .... _-_ ............... _ ........•. _ ..... __ ._ ..... _ ... _-.............. __ ...... _ ..... _ ........ _-_........... . -_._----_. ---------._--_._. __ ._-_._--_._--_.-. . ..... -.......................... __ ...... _-_ ... __ ............ _--_ ...... __ ... __ ........ __ ............. -.. __ ......... _-_ ............ _.-.... -.... -... _.-....... -.. _._.-.-.--.-.---.--_._-------------------_._._-------._------_._._._._----_. __ ._--_._-_. __ ._----_. __ .•. _---_ .. __ .. __ ._ .. _ ..... _._-_._ ... _._ ... __ ._--_. __ ._ .. __ ._ .. _ ... _ ... _-_ ... _ ........ __ ._ .. _ ... _ .. _ .. __ ._-_ ... _--------_._._-----_._------_._._-_._-_._--------_._-----------_._. __ .. __ .. _.-...... _ ... _ ...... _ ... _ ............................... . ----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------_.---------_._ ... _._._._-_ ... _ ..... _ ........ _ ......... _ ... _ ............. _ ... _ ............. _ ... _ ................. _ .... _ ............. - 1.00E-17 ~ C\I C") "'¢ l.C) CD I"-co 0> 0 ~ C\I C") "'¢ l.C) CD I"-co 0> 0 ~ C\I C") "'¢ l.C) CD I"-co 0> 0 co co co co co co co co co 0> 0> 0> 0> 0> 0> 0> 0> 0> 0> 0 0 0 0 0 0 0 0 0 0 ~ ~ I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. 0. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) -E :::: (J ::l - ~ ~ I W 0 ~ ~ N ("f) ~ ~ I I W W 0 0 ~ ~ .;:t ~ I W 0 0 ... ~ ! ~-- iii I I !.o:==~ ~: t :~ ~ ,I,,· i i i--I-Li.J i i jl ~ : . jl1 1 I L I Ii! i ! r~ll!i Ii k ~ll L{) ~ I W 0 ~ (eleos 501) ~ ~ ~-des o~-des 60-deS go-des LO-deS go-des go-des Po-des £O-deS lO-deS ~o-des OO-deS 66-deS 96-deS L6.,.deS 96-deS 96-deS P6-deS £6-deS l6-deS ~6-des 06-deS 69-deS gg-deS L9-deS gg-deS gg-deS pg-des £g-deS 19-deS ~g-des c.o r-.... ~ ~ I I W W 0 0 ~ ~ ~ 1.00E-11 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCilml Pre 1994 ALARA Goal = 1 E-12 uCi/ml BHV-5 Lead-210 Concentrations (uCi/ml) , 1~~~2 ~~~~_~~~~~_~~ __ ~~~~ __ 1 ___________ ~ _____ ~ _____ --~~ , 1 . OOE-13 _______________________________ . __________________ ._. _____________ . _______________ . ________________________________ _ CD ro u CI.I .OOE-14 0) o ~ .... ,._--_._----_._-_ .. _-----,._-_._._----_ ... _--_._---.---------------------------------------_ .. _--------------------_ .. _-.. _-------_._ .. ,._--------------.......................... __ ...... __ .. . -----------------------------_._---_._----_._-_._------........ _ ........ _ .... _ ....... _ ...... __ ... _ ... _ ... __ .. --_._-_ .... _--_._-------_._-_ ...... _-------_._-----------------................ _ ... __ .-.-_ .. _ ... _ .... _-...... -..•......•....•..... __ .... -.........•..•..•.•.....•... -......... -..... .._-._. -------... , .. -...... _ ... . ------------------------_._-----+ ............................................................... _ ...... _ ......... . ---------------------------------....... ---... -........ -... -··········1 1.00E-15 _ l ~ • M ::::::::::>-:-:-----:::-~~~~~~:=:=:::-:=:=:=:~~d 1.00E-16 g~~~~§~~~~~~~~~§~~~~~~~~~~~~~~~~~~~~~~§ 1.00E-17 T""" N (") ~ L() co ""'"" co C') 0 T""" N (") ~ L() co ""'"" co C') 0 T""" N (") ~ L() co ""'"" co C') 0 co co co co co co co co co C') C') C') C') C') C') C') C') C') C') 0 0 0 0 0 0 0 0 0 0 T""" T""" I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. a. Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) Q) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) TAB 6 BHV-6 AIR SAMPLING GRAPHS AND DATA TABLE Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-6U Effluent Concentration Limit = 2E-14 uCi/ml BHV-6T Effluent Concentration Limit = 9E-13 uCi/ml BHV-6R Effluent Concentration Limit = 6E-13 uCi/ml BHV-6PB ALARAGoal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 9/28/1981 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 12/14/1981 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 3/29/1982 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 6/30/1982 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 9/27/1982 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 1/3/1983 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 4/4/1983 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 6/30/1983 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 10/3/1983 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 1/3/1984 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 4/2/1984 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 7/2/1984 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 10/1/1984 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 1/2/1985 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 4/1/1985 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 7/1/1985 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 9/30/1985 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 1/2/1986 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 4/1/1986 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 6/30/1986 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 10/27/1986 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 12/15/1986 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 3/16/1987 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 5/11/1987 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 9/9/1987 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 11/2/1987 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 2/16/1988 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 5/18/1988 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 8/15/1988 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 11/14/1988 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 2/13/1989 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 5/15/1989 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 8/14/1989 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 11/13/1989 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 2/12/1990 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 5/14/1990 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 8/13/1990 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 11/12/1990 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 2/11/1991 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 5/13/1991 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 8/12/1991 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 11/11/1991 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 2/10/1992 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 5/11/1992 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 8/10/1992 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 11/9/1992 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 2/9/1993 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 5/10/1993 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 8/10/1993 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 11/8/1993 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 2/7/1994 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 5/9/1994 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 8/9/1994 s.OOE-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 11/7/1994 s.00E-12 1.2sE-12 8.00E-14 2.00E-14 2.00E-12 s.OOE-13 4.00E-12 1.00E-12 2/7/1995 9.00E-14 2.2sE-14 2.00E-14 s.00E-1s 9.00E-13 2.2sE-13 6.00E-13 l.s0E-13 5/9/1995 9.00E-14 2.2sE-14 2.00E-14 s.OOE-1s 9.00E-13 2.2sE-13 6.00E-13 l.s0E-13 8/9/1995 9.00E-14 2.2sE-14 2.00E-14 s.00E-1s 9.00E-13 2.2sE-13 6.00E-13 l.s0E-13 Date Effluent Concentration limit = 9E-14 uCi/ml BHV-6U Effluent Concentration limit = 2E-14 uCi/ml BHV-6T Effluent Concentration limit = 9E-13 uCi/ml BHV-6R Effluent Concentration limit = 6E-13 uCi/ml BHV-6PB ALARAGoal = 2.2SE-14 uCi/ml ALARA Goal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC limit = SE-12 uCi/ml Pre 1994 MPC limit = 8E-14 uCi/ml Pre 1994 MPC limit = 2E-12 uCi/ml Pre 1994 MPC limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 11/11/199S 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 2/S/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 1.S0E-13 S/6/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 8/S/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 1.S0E-13 11/6/1996 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 1.50E-13 2/6/1997 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 S/S/1997 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 8/11/1997 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 1/S/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 4/28/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 7/31/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 9/28/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 12/28/1998 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 l.S0E-13 3/29/1999 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 1.S0E-13 7/3/1999 9.00E-14 2.2SE-14 2.00E-14 S.00E-1S 9.00E-13 2.2SE-13 6.00E-13 1.50E-13 9/27/1999 3.03E-1S 9.00E-14 2.2SE-14 1.37E-1S 2.00E-14 S.00E-1S 8.72E-16 9.00E-13 2.2SE-13 7.SSE-1S 6.00E-13 1.S0E-13 12/28/1999 S.01E-1S 9.00E-14 2.2SE-14 2.89E-1S 2.00E-14 S.00E-1S l.3lE-1S 9.00E-13 2.2SE-13 8.10E-1S 6.00E-13 l.S0E-13 3/30/2000 7.46E-16 9.00E-14 2.2SE-14 S.2SE-16 2.00E-14 S.00E-1S 3.00E-16 9.00E-13 2.2SE-13 7.83E-1S 6.00E-13 l.S0E-13 6/26/2000 S.40E-16 9.00E-14 2.2SE-14 3.S3E-16 2.00E-14 S.00E-1S 6.11E-16 9.00E-13 2.2SE-13 4.83E-1S 6.00E-13 1.S0E-13 9/2S/2000 3.7SE-16 9.00E-14 2.2SE-14 2.23E-16 2.00E-14 S.00E-1S 1.91E-16 9.00E-13 2.2SE-13 6.4lE-1S 6.00E-13 l.S0E-13 12/26/2000 S.21E-16 9.00E-14 2.2SE-14 3.39E-16 2.00E-14 S.00E-1S 3.2SE-17 9.00E-13 2.2SE-13 8.S7E-1S 6.00E-13 l.S0E-13 3/26/2001 1.42E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.1SE-1S 6.00E-13 l.S0E-13 7/2/2001 1.8lE-16 9.00E-14 2.2SE-14 1.66E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.9SE-1S 6.00E-13 l.S0E-13 9/24/2001 3.08E-16 9.00E-14 2.2SE-14 1.01E-16 2.00E-14 S.00E-1S 1.77E-16 9.00E-13 2.2SE-13 8.S9E-1S 6.00E-13 l.S0E-13 12/31/2001 3.3lE-16 9.00E-14 2.2SE-14 1.2SE-16 2.00E-14 S.00E-1S 1.09E-16 9.00E-13 2.2SE-13 3.14E-1S 6.00E-13 l.S0E-13 4/1/2002 4.77E-16 9.00E-14 2.2SE-14 2.94E-16 2.00E-14 S.00E-1S 1.96E-16 9.00E-13 2.2SE-13 8.61E-1S 6.00E-13 1.S0E-13 7/1/2002 3.68E-16 9.00E-14 2.2SE-14 4.41E-16 2.00E-14 S.00E-1S 1.76E-16 9.00E-13 2.2SE-13 8.20E-1S 6.00E-13 l.S0E-13 9/30/2002 3.67E-16 9.00E-14 2.2SE-14 S.60E-16 2.00E-14 S.00E-1S 1.80E-16 9.00E-13 2.2SE-13 S.SSE-1S 6.00E-13 1.S0E-13 12/30/2002 1.00E-16 9.00E-14 2.2SE-14 3.43E-16 2.00E-14 S.00E-1S 1.67E-16 9.00E-13 2.2SE-13 l.3SE-14 6.00E-13 l.S0E-13 3/31/2003 1.98E-16 9.00E-14 2.2SE-14 1.6SE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 7.77E-1S 6.00E-13 l.S0E-13 6/30/2003 1.18E-16 9.00E-14 2.2SE-14 1.1SE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.92E-1S 6.00E-13 l.S0E-13 9/29/2003 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 8.30E-1S 6.00E-13 l.S0E-13 12/29/2003 1.00E-16 9.00E-14 2.2SE-14 1.36E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.66E-1S 6.00E-13 1.S0E-13 3/29/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 8.17E-1S 6.00E-13 1.S0E-13 6/27/2004 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 3.SSE-1S 6.00E-13 l.S0E-13 9/27/2004 1.00E-16 9.00E-14 2.2SE-14 l.38E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.22E-14 6.00E-13 l.S0E-13 12/27/2004 1.0SE-16 9.00E-14 2.2SE-14 1.72E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 l.S2E-14 6.00E-13 l.S0E-13 3/28/200S 1.00E-16 9.00E-14 2.2SE-14 1.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 9.34E-1S 6.00E-13 l.S0E-13 6/29/200S l.28E-16 9.00E-14 2.2SE-14 1.01E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 9.8SE-1S 6.00E-13 l.S0E-13 9/26/200S 1.98E-16 9.00E-14 2.2SE-14 S.9SE-16 2.00E-14 S.00E-1S 3.SSE-16 9.00E-13 2.2SE-13 1.71E-14 6.00E-13 1.S0E-13 1/3/2006 7.67E-16 9.00E-14 2.2SE-14 2.88E-16 2.00E-14 S.00E-1S 3.60E-1S 9.00E-13 2.2SE-13 4.8SE-14 6.00E-13 l.S0E-13 4/3/2006 2.92E-16 9.00E-14 2.2SE-14 2.00E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.11E-14 6.00E-13 1.S0E-13 7/3/2006 3.2SE-16 9.00E-14 2.2SE-14 2.36E-16 2.00E-14 S.00E-1S 1.0SE-16 9.00E-13 2.2SE-13 1.10E-14 6.00E-13 1.S0E-13 10/2/2006 S.03E-16 9.00E-14 2.2SE-14 1.49E-16 2.00E-14 S.00E-1S 1.19E-16 9.00E-13 2.2SE-13 2.13E-1S 6.00E-13 1.S0E-13 1/1/2007 8.31E-16 9.00E-14 2.2SE-14 2.49E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.70E-14 6.00E-13 l.S0E-13 4/2/2007 S.36E-16 9.00E-14 2.2SE-14 3.1SE-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 1.43E-14 6.00E-13 l.S0E-13 7/2/2007 1.08E-1S 9.00E-14 2.2SE-14 2.18E-16 2.00E-14 S.00E-1S l.S4E-16 9.00E-13 2.2SE-13 2.04E-14 6.00E-13 l.S0E-13 9/30/2007 3.92E-16 9.00E-14 2.2SE-14 1.02E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 6.38E-1S 6.00E-13 l.S0E-13 12/31/2007 2.92E-1S 9.00E-14 2.2SE-14 l.SSE-1S 2.00E-14 S.00E-1S 3.16E-16 9.00E-13 2.2SE-13 9.19E-1S 6.00E-13 l.S0E-13 3/31/200S 4.34E-16 9.00E-14 2.2SE-14 3.S1E-16 2.00E-14 S.00E-1S 1.00E-16 9.00E-13 2.2SE-13 S.99E-1S 6.00E-13 1.S0E-13 6/3102008 1.88E-1S 9.00E-14 2.2SE-14 9.00E-16 2.00E-14 S.00E-1S 4.04E-16 9.00E-13 2.2SE-13 7.41E-1S 6.00E-13 l.S0E-13 9/30/2008 4.82E-1S 9.00E-14 2.2SE-14 2.10E-1S 2.00E-14 S.00E-1S 1.27E-1S 9.00E-13 2.2SE-13 1.00E-14 6.00E-13 l.S0E-13 12/31/2008 4.S0E-1S 9.00E-14 2.2SE-14 l.70E-1S 2.00E-14 S.00E-1S 1.2SE-1S 9.00E-13 2.2SE-13 1.49E-14 6.00E-13 1.S0E-13 3/1S/2009 2.77E-1S 9.00E-14 2.2SE-14 1.0lE-1S 2.00E-14 S.00E-1S 7.S2E-16 9.00E-13 2.2SE-13 6.46E-1S 6.00E-13 1.S0E-13 6/1S/2009 1.41E-16 9.00E-14 2.2SE-14 2.67E-16 2.00E-14 S.00E-1S 1.8lE-16 9.00E-13 2.2SE-13 S.76E-1S 6.00E-13 l.S0E-13 9/1S/2009 4.87E-1S 9.00E-14 2.2SE-14 4.32E-16 2.00E-14 S.00E-1S 2.23E-16 9.00E-13 2.2SE-13 8.98E-1S 6.00E-13 l.S0E-13 12/1S/2009 9.24E-1S 9.00E-14 2.2SE-14 2.26E-16 2.00E-14 S.00E-1S 1.1SE-16 9.00E-13 2.2SE-13 6.44E-1S 6.00E-13 l.S0E-13 Date Effluent Concentration Limit = 9E-14 uCi/ml BHV-6U Effluent Concentration Limit = 2E-14 uCi/ml BHV-6T Effluent Concentration Limit = 9E-13 uCi/ml BHV-6R Effluent Concentration Limit = 6E-13 uCi/ml BHV-6PB ALARA Goal = 2.2SE-14 uCi/ml ALARAGoal = SE-13 uCi/ml ALARAGoal = 2.2SE-13 uCi/ml ALARAGoal = 1.SE-13 uCi/ml Pre 1994 MPC Limit = SE-12 uCi/ml Pre 1994 MPC Limit = 8E-14 uCi/ml Pre 1994 MPC Limit = 2E-12 uCi/ml Pre 1994 MPC Limit = 4E-12 uCi/ml Pre 1994 ALARA GOAL = 1.2SE-12 uCi/ml Pre 1994 ALARA GOAL = SE-13 uCi/ml Pre 1994 ALARA GOAL = 1E-12 uCi/ml Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA Cone EFC EFCA 3/31/2010 9.63E-1S 9.00E-14 2.2SE-14 1.82E-16 2.00E-14 S.00E-1S 2.06E-16 9.00E-13 2.2SE-13 L37E-14 6.00E-13 LSOE-13 6/30/2010 3.62E-1S 9.00E-14 2.2SE-14 3.94E-16 2.00E-14 S.00E-1S 4.89E-16 9.00E-13 2.2SE-13 4.30E-1S 6.00E-13 LSOE-13 9/30/2010 S.42E-1S 9.00E-14 2.2SE-14 L08E-1S 2.00E-14 S.00E-1S S.68E-16 9.00E-13 2.2SE-13 3.98E-1S 6.00E-13 1.S0E-13 12/31/2010 L24E-14 9.00E-14 2.2SE-14 1.2lE-1S 2.00E-14 S.OOE-IS 1.00E-1S 9.00E-13 2.2SE-13 1.S3E-14 6.00E-13 LSOE-13 4/4/2011 2.70E-1S 9.00E-14 2.2SE-14 4.62E-16 2.00E-14 S.00E-1S 6.SlE-16 9.00E-13 2.2SE-13 1.29E-14 6.00E-13 LSOE-13 7/4/2011 3.0lE-1S 9.00E-14 2.2SE-14 7.07E-16 2.00E-14 S.OOE-IS S.7SE-16 9.00E-13 2.2SE-13 7.97E-1S 6.00E-13 LSOE-13 10/3/2011 2.0SE-1S 9.00E-14 2.2SE-14 6.12E-16 2.00E-14 S.00E-1S L88E-16 9.00E-13 2.2SE-13 9.93E-1S 6.00E-13 LSOE-13 1/3/2012 3.14E-IS 9.00E-14 2.2SE-14 L09E-IS 2.00E-14 S.00E-1S 7.6SE-16 9.00E-13 2.2SE-13 L89E-14 6.00E-13 LSOE-13 4/3/2012 4.4lE-lS 9.00E-14 2.2SE-14 L82E-1S 2.00E-14 S.00E-1S 4.00E-16 9.00E-13 2.2SE-13 LSOE-14 6.00E-13 1.50E-13 7/2/2012 6.42E-IS 9.00E-14 2.2SE-14 2.2SE-1S 2.00E-14 S.00E-1S S.11E-16 9.00E-13 2.2SE-13 9.S4E-IS 6.00E-13 LSOE-13 -E :::: U :::l - ~ ~Oll£IO ~ 900l10£/6 900l19l16 o T""" N I "'0 CO lOOlIO£/6.3 t <0 N N 666~lLl16 E 966~/9/9 :J :.c CO 0:: t o C") N E :J ·c o £66~/O~/9~ t ro ~ 066~/£~/9~ z E .~ c CO ~ :J L96~/6/6 t 1796 ~/~/O ~ 1.00E-11 Effluent Concentration Limit = 9E-14 uCi/ml ALARA Goal = 2.2SE-14 uCi/ml Pre 1994 MPC Limit = SE-12uCi/ml Pre 1994 ALARA Goal = 1.2SE-12 uCi/ml BHV-6 Uranium-Natural Concentrations (uCi/ml) ;;=-==:======='=-==-='='='=~~~~~~~~~~~='~~='~~='~='~~='~~'~~~~~~~~~~~~~~~~~~~ 1 .OOE-12 ~ ----. _. --t -----_. -. . --. ... .. --~ __________ ._. ______ •• ___ •• __ • ___ • ___ • ____ • _________ • __________ • ___ ••••••••• __ • ______ • _______________ • __ •• __ •• __ ....... no_ "'n _____ • ____ ."___ "'n" ___ "' __ "___ ••• n_ •••••••• _ •• _ •••• _________ • '_n_"_""_' __ ' __ ' ____ '____ •• ______ •• ___ .... _________ • ______ •• ___ .... _. __ • _____ •••• _. __ ••• " __ • __ ._ •••• _. ___ • __ ._ •••• _ •••••• __ ••• __ • ___ ••• _______ ._ ...... __ ............. ____ • __ •••••••••• _____ •••••••••• _____ ••. __ ••••• m ............... __ ••••••••••••• __ ••••••••••••• __ ••• __ •••• _m __ ............. __ ••• __ ••••••••••••• __ .......................... _ ................... _ •••• 1.00E-13 ~ _... . ----. ---t · Q) CO I c?l.OOE-1 4 t C) I I • o .... ,., I" :::::... 1£ ~ "I • .J..I I \ • \ .... ..l T I T ~ T ' T 1n~~5 __ ~ ________ ~_~~ ________ ~~ __ ~ ______________ ~ ______ ~~ _________ _ 1n~~6 ~~~~~~.~~~~ ~ -------------------------------------------------------------------------------------------------------------------_._--_._----_._-._-------.. _._-_ .. __ .. _ .. _--_ .. _._ .. _ .. __ ._ ........ _-_ ..•... _._. __ .-. _ .. _ .... _ .. _ .. _ .. _ ......... _ .. _ .............. _ ............. _ .......... _-_ .... . ----------------------------------------------_ .. _--------------------_._--------------------_._--_._-------._-_. __ .. _. __ ._._._ ... _._ ... _ .. _--_ .. _ .. __ ._--............................................... -.................................................................................................................................. _ ...... . ------------------------------------------------------------------------------------------------------------------------------------------------------_._ ...•. __ ._ .. __ ... _--_._ ... _._._ .. - 1.00E-17 T"" "d" I"-0 ('t') CO 0) N L!) 00 00 00 00 0) 0) 0) 0) 0 0 0 T"" 0) 0) 0) 0) 0) 0) 0) 0 0 0 0 T"" T"" T"" T"" T"" T"" T"" N N N N - --- -- - - - - -00 T"" 0) ('t') 0 L!) I"-0 CO 0 ('t') N --T"" T"" -N ('t') N ('t') --0 0) - - 00 - - - - 0 0) 00 00 0) 0) 0) 0) 1.00E-11 Effluent Concentration Limit = 2E-14 uCilml ALARA Goal = 5E-13 uCi/ml Pre 1994 MPC Limit = 8E-14uCi/ml BHV-6 Thorium-230 Concentrations (uCi/ml) 1.00E-12 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ CD -.... -.-.-.. --.--.-__ ._ .. __ ::::_._._._._.___. ___ ._ .. ___ .. __ ... _._._ .... _._._ .. __ _ __ .... __ .. ____ ... ____ . __ _ Iii _________ _ ~.OOE-14 --------_---~::~::~:-:------_--~ __ 2- o 11 1 .00 E -1 5 __ . _____ :~~=~=~=~:::_~:::::=~=~=~=~=~~--.::==---==-=-==-=-.:::::~=~=~=~=~=~=~~~~-.-.--=--=--=-.:::::=:~:=:~_=.:::_=.:::-==~:=:~=:=.::_:.::-.::::-~:::-.::.::-.:::::-.::-.:::.:::~:::-.::==.:::.:::-====~~:~~:::~~= ._=~-:.::_~::.::.=.::=~_==_-=::::::::::::===:===:_::::::~:_=:_::::::~:::==_ ----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------_ ... _----------------------_.-... __ ... __ ._. __ ... __ ._ ... _---_._--_ ... __ ._ ... _._ .. _._.---.--.-~ .... __ . __ . __ ._._--_ ... _ ... _--.... _ ..... _. __ . __ . __ ._ ... _-_ ... _. __ ._--_ ... _ ... _ ... __ ._ ... __ .. 1 .00 E -16 _~;~;_;_=~~~~~_~~~_~_~~~~_~~~_~~~_~~~~==_=_~~~~~~~~_~~~~~~~~;::;_~~~~~~~~~~~~~~~~~~~~~~~~~~~~.::~~~~::~~~~=_::~:~~~~::::~~::=~::~~=~~-~::~~~:::~_~_~:::=::~=_~=:=:~~.---.............. :~~~=~===~_~=::~==:==::~~=:==:=~==:~=~==::::::::::======---.. --_. _______________ ._ ------------------------------------------------------------------------------------------=---~-~~-~--=---~-~.-~~-~.-~:-~---~-~~-:==~-~~:~~===~--===~~~=-............................................................................................................................................................................................................. _ ... . 1.00E-17 ~ ~ ~ I'-0 ('f) co C) N LC') co ~ co co co C) C) C) C) 0 0 0 ~ C) C) C) C) C) C) C) 0 0 0 0 ~ ~ ~ ~ ~ ~ ~ N N N N ---- ----- - - co ~ C) ('f) 0 LC') I'-0 co 0 ('f) N --~ ~ -N ('f) N ('f) --0 C) - - co --- - 0 C) co co C) C) C) C) 1.00E-11 Effluent Concentration Limit = 9E-13 uCi/ml ALARA Goal = 2.25E-13 uCi/ml Pre 1994 MPC Limit = 2E-12uCi/ml Pre 1994 ALARA Goal = 5E-13 uCi/ml \ 1 .00 E -12 1:::::::::::::::._ ... __ ... ___ . _____ ._. __ . ______ ... _____ . _____ . _______________ . ____ . _____ ... __ . __ . ___ ... __ . __ ._._ .. _. __ . __ . __ ... _ ... _ ........................... _ ...... _ BHV-6 Radium-226 Concentrations (uCi/ml) r---.. -.------.---.-----------------.----.-.------------------.---------------------------------. ...... __ ._ ... _ .. _. __ .. _ ......... -.. _ ... _ .. __ ._-._ .. --------_._-_._--_._-_._----------_._------_._--_._--_._------_._------............................................. -................................................................................. -............................... -._ ... -._--_ .... _._-----------_._--_ .. _-----_._--_._-.............. ..=:::====\-= .. _--..•...•. ~ .•.... :::::::::.:.. ............................................ . --------------------------------------------------------------------------------------------------_ ... _- 1.00E-13 g~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~@ Q) ro bj .00E-14 0) o ...J -. 1 .00 E -1 5 ... _ .. _ ........ _ ... _ ... _._ ..... _ .............. _ ........ _ ... _._ ........... _ ..... _ .... _ .. _ ...... __ .... _ .. _ ... _ .. __ ..... _. ___ ...... _. ______ ._ .. _. __ ... _._ ............................................................... _ ... -......... -... -.... _ ...•. _ ..•...•..•...........•..•...•..•..............•..•...•.......•..•...•....•..•.. _ ..•..•. _._._ ..•..•. -................................................................. -..................................................................................... _. ----------------------------------------------------------------_ ... ----_ .. _ ... _. __ ._-_ .•. _ ... _. __ . __ . __ ._--_. __ ._ ••.•. _-_. __ ... -... _ .•. __ . __ .•. _-_ .•..•. __ .•. _-_. __ . __ .-_ .•. _. __ ._ ••.•. _ .•. _. __ .•. _. __ . __ ... _._ ..... _ ... _. __ ... _ ... _ ... _ ... _ ............. _ ........ _ ... - .................................. -............................................. -.................................... _ ................................................. _. -----------------------------_._-----------------------_._----------------------------------------------------------------_._--_. 1 .00 E -1 6 . ___ . ______ . __ . ____ ... _. __ . __ . __ . _____ ... _._ ... _. __ ... _._. __ ... ___ ... _ .. _. __ ... _. __ ... _ ... _ ........ _ ... _ ... _ ... _ ... _ ... _ ....... _ ... _ ... _ ... _ ........ _ ... _ ......... _ ... __ ._--_ ... _-_. __ ... __ ...... _ ... __ ._ .. _ ... _ ... __ . __ .......... _ ..... __ ...................... _ ... __ ........ _._ ... _ ............................ _ ................ _ ............. _ ............ _ .. _ ........ -............................. _ ... . ---------_ .. _-----------------------------------------------_ ... _ .. _--_ .. __ ._-_ ..... _._--_ ... _._------_ ..... _--_.---..... --_ .. -.•.. __ .-..... . ..... _ ... _ .. _--_._ .. _ .... - \j 4 1.00E-17 TTTT ~ .:::t I'--0 C") co 0) N L() 00 00 00 0) 0) 0) 0) 0 0 0) 0) 0) 0) 0) 0) 0) 0 0 ~ ~ ~ ~ ~ ~ ~ N N --- - - - ---00 ~ 0) C") 0 L() I'--0 co N --~ ~ -N C") N -0 0) - - 00 -- - 0) 00 00 0) 0) 0) 00 ~ 0 ~ 0 0 N N - -0 C") C") --0 0) 1.00E-11 Effluent Concentration Limit = 6E-13 uCi/ml ALARA Goal = 1.5E-13 uCi/ml Pre 1994 MPC Limit = 4E-12uCi/ml Pre 1994 ALARA Goal = 1 E-12 uCi/ml BHV-6 Lead-210 Concentrations (uCi/ml) , I 1.00E-12 ~-=====-c::==~~~::=~~~~~~=t~~~~~~~~~:~~:~~:~~~~~~~~~~~.~;~~~ I I 1.00E-13 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ T 1\ J 1.00E-15 E~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-16 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-17 --rrrr 'r" ~ r-..... 0 C"') <0 0) C\I L.() co co co co 0) 0) 0) 0) 0 0 0 'r" 0) 0) 0) 0) 0) 0) 0) 0 0 0 0 'r" 'r" 'r" 'r" 'r" 'r" 'r" C\I C\I C\I C\I ------ -- -- - co 'r" 0) C"') 0 L.() r-..... 0 <0 0 C"') C\I --'r" 'r" -C\I C"') C\I C"') --0 0) - - co - ---0 0) 'r" co co 0) 0) 0) 0) ATTACHMENT C AIR PARTICULATE LABORATORY RESULTS AND QAIQC www.energylab.com 'E"-ERGY LABORATORIES AI18/ytical Ext:81l1H1CB Sincs 1952 f Helena, MT 877-472-0711 -Billings, MT 800-135-4489 -Casper, WY8S8-235-05l5 Gillette, WY866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX888-690-2218 ANALYTICAL SUMMARY REPORT May 27,2012 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C12040316 Project Name: 1 st Quarter Air 2012 Energy Laboratories, Inc. Casper WY received the following 6 samples for Denison Mines USA Corp on 4/6/2012 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C12040316-001 BHV-1 04/03/12 00:00 04/06/12 Filter Composite of two or more samples Metals, Total Digestion, Total Metals Lead 210 Radium 226 Thorium, Isotopic C 1204031 6-002 BHV-2 04/03/12 00:00 04/06/12 Filter Sam e As Above C 1204031 6-003 BHV-4 04/03/12 00:00 04/06/12 Filter Same As Above C 1 2040316-004 BHV-5 04/03/12 00:00 04/06/12 Filter Same As Above C 12040316-005 BHV-6 04/03/12 00:00 04/06/12 Filter Same As Above C 1204031 6-006 Biankl2A 04/03/12 00:00 04/06/12 Filter Sam e As Above The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 , unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. Data corrected for moisture content are typically noted as - dry on the report. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. If you have any questions regarding these test results, please call. Report Approved By: Digitally signed by Steve Carlston Date: 2012.05.27 15:08:40 -06:00 Page 1 of 22 www.energyiab.com Analytfcal Ext;8llsncB Since 1952 Helena, MT 877-472-0711 • Billings" MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College station, IX 888-690-2218 CLIENT: Denison Mines USA Corp Project: 1 st Quarter Air 2012 Report Date: OS/27/12 Sample Delivery Group: C12040316 CASE NAR RATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Virginia: 00057; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. Page 2 of 22 EN:RGY LABORATORIES www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-412-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-1175 • Rapid City, SO 888-612-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 27, 2012 PROJECT: 1st Quarter Air 2012 SAMPLE ID: BHV-1 QuarterlDate Sampled RadionucIide Concentration Air Volume JlCilmL C 12040316-00 1 natu 7.87E-16 First Quarter 2012 230Th 2.64E-16 Air Volume in mLs 226Ra 3.95E-16 1.37E+11 210pb 1.25E-14 +LLD's are from Reg. Guide 4.14 Counting Precision JlCilmL N/A 3E-17 1E-17 1E-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDC JlCilmL N/A 6E-18 3E-18 4E-17 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration 1E-16 9E-14 8.75E-01 1E-16 3E-14 8.80E-Ol 1E-16 9E-13 4.39E-02 2E-15 6E-13 2.08E+OO Page 3 of 22 ------===-i~N i~ EN:RGY L.ABORATORIES www.energylab.com Analytical fxcsllsncB SiIlCB 7852 Helena, MT 877 .. 412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY866-686-7175 • Rapid City, SI) 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 1 st Quarter Air 2012 C12040316-001 Client Sample 10 BHV-1 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES . l ead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.159 107 1700 16 5.4 53.9 1.4 0.4 36 4.4 0.77 MOC -Minimum detectable concentration Units mglfilter pC ilFi Iter pCilFilter pCilFilter pCilFilter pC ilFi Iter pC ilFi Iter pC ilFi Iter pCilFilter pCilFilter pCilFilter Qualifiers Rl 0.0003 0.2 Report Date: 05/27/12 Collection Date: 04/03/12 DateReceived: 04/06/12 Matrix: Filter MCL! QCl Method Analysis Date / By SW6020 04/11/12 07:49 1 smm SW6020 04/11/1207:49/ smm E909.0 04/28/12 01 :39 1 eli-cs E909.0 04/28/1201 :39 1 eli-cs E909.0 04/28/12 01 :39 / eli-cs E903.0 05/15/12 00:23 1 trs E903.0 05/15/12 00:23 1 trs E903.0 05/15/12 00:23 1 trs E908.0 04/17/12 17:231 dmf E908.0 04/17/1217:231 dmf E908.0 04/17/12 17:231 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 22 EN:RGY L ABORATORIES www.energylab.com Ana/ftical Excellence Since 1952 Helena, MT 817-412-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7115 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 27, 2012 PROJECT: 1st Quarter Air 2012 SAMPLE ID: BHV-2 QuarterlDate Sampled RadionucIide Concentration Air Volume fl CilmL C 12040316-002 natU 4.22E-16 First Quarter 2012 230Th 1.15E-16 Air Volume in mLs 226Ra 2.77E-16 1.37E+ll 210Pb 1.58E-14 +LLD's are from Reg. Guide 4.14 Counting Precision flCilmL N/A 2E-17 9E-18 lE-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDCflCilmL N/A 4E-18 3E-18 4E-17 L.L.D.+ Effluent Cone. * % Effluent flCilmL flCilmL Concentration lE-16 9E-14 4.68E-Ol lE-16 3E-14 3.84E-Ol lE-16 9E-13 3.07E-02 2E-15 6E-13 2.63E+00 Page 5 of 22 EN:RGY LABORATORIES www.energylab.com r' Analytical Exesllsocs SiI1C8 1952 ). Helena, MT 877 .. 472-0711 -Billings, MT 800-735-4489 . Casper, WY 888-235-0515 Gillette, wv866-686-711S • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 1 st Quarter Air 2012 C12040316-002 Client Sample 10 BHV-2 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0850 57.6 2150 18 5.4 37.8 1.2 0.4 16 2.3 0.58 MOC -Minimum detectable concentration Units mglfilter pCilFilter pCilFilter pC ilFi Iter pC ilFi Iter pC ilFi Iter pCilFilter pC ilFi Iter pCilFilter pCilFilter pCilFilter Qualifiers Rl 0.0003 0.2 Report Date: 05/27/12 Collection Date: 04/03/12 DateReceived: 04/06/12 Matrix: Filter MCL! QCl Method Analysis Date 1 By SW6020 04/11/12 07:51 1 smm SW6020 04/11/1207:51 1 smm E909.0 04/28/1203:541 eli-cs E909.0 04/28/12 03:541 eli-cs E909.0 04/28/12 03:541 eli-cs E903.0 05/15/1200:231 trs E903.0 05/15/12 00:231 trs E903.0 05/15/12 00:23 1 trs E908.0 04/17/12 17:241 dmf E908.0 04/17/1217:24/dmf E908.0 04/17/12 17:241 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 22 -------~. www.energylab.C1lm r---Helena.MT817-412-0711 .Biliings.MT 800-735-4489 • Casper, WY 888-235-0515 ~ Analytical Excellence Since 1952 ) Gillette, WY 866-686-1175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 ,EN:RGY LABORATORIES ~-=============~~----~----------~--~----------~----------- HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 27, 2012 PROJECT: 1st Quarter Air 2012 SAMPLE ID: BHV-4 QuarterlDate Sampled RadionucIide Concentration Air Volume ,..CilmL C12040316-003 natU 2.51E-15 First Quarter 2012 230Th 5.02E-16 Air Volume in mLs 226Ra 2.27E-16 1.36E+11 210Pb 1.03E-14 +LLD's are from Reg. Guide 4.14 Counting Precision ,..CilmL N/A 6E-17 8E-18 1E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-210 MDC,..CilmL N/A 9E-18 3E-18 4E-17 L.L.D.+ Effluent Cone. * % Effluent ,..CilmL ,..CilmL Concentration 1E-16 9E-14 2.79E+00 1E-16 3E-14 1.67E+00 1E-16 9E-13 2.52E-02 2E-15 6E-13 1.72E+00 Page 7 of 22 EN:RGY LABORATORIES www.energylab.com Analytical Exesllsnes SiI1ClJ .,m ~--~------------------------------------------Helena, MT 877 ~4 72-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-1175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 1st Quarter Air 2012 Lab ID: C 12040316-003 Client Sample ID BHV-4 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.506 342 1410 15 5.4 30.9 1.0 0.4 68 7.9 1.3 MOC -Minimum detectable concentration Units mg/filter pCilFilter pC ilFi Iter pC ilFi Iter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter pC ilFi Iter pC ilFi Iter Qualifiers RL 0.0003 0.2 Report Date: 05/27/12 Collection Date: 04/03/12 DateReceived: 04/06/12 Matrix: Filter MCU QCL Method Analysis Date / By SW6020 04/11/1220:331 cp SW6020 04/11/1220:331 cp E909.0 04/28/12 06:09 1 eli-cs E909.0 04/28/12 06:09 1 eli-cs E909.0 04/28/12 06:09 1 eli-cs E903.0 05/15/12 12:43 1 trs E903.0 05/15/12 12:43 1 trs E903.0 05/15/12 12:43 1 trs E908.0 04/17/12 17:241 dmf E908.0 04/17/12 17:24 1 dmf E908.0 04/17/12 17:241 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 8 of 22 EN:RGY LABORATORIES www.energylab.com Analytical Excellence Since 1952 Helena, MT 817-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 27, 2012 PROJECT: 1st Quarter Air 2012 SAMPLE ID: BHV-5 QuarterlDate Sampled Radionuclide Concentration Air Volume flCilmL C12040316-004 natu 5.52E-15 First Quarter 2012 230Th 3.24E-15 Air Volume in mLs 226Ra 1.79E-15 1.36E+11 210Pb 1.55E-14 +LLD's are from Reg. Guide 4.14 Counting Precision flCilmL N/A 3E-16 2E-17 1E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDC flCilmL N/A 2E-17 3E-18 4E-17 L.L.D.+ Effluent Cone. * % Effluent flCilmL flCilmL Concentration 1E-16 9E-14 6. 13E+OO lE-16 3E-14 1.08E+Ol 1E-16 9E-13 1.99E-01 2E-15 6E-13 2.58E+00 Page 9 of 22 EN:RGY LABORATORIES www.energylab.com Analytical Excsllsnce SiIlCS 1!152 r . Helena, MT 877-472-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-1175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 1 st Quarter Air 2012 Lab ID: C 12040316-004 Client Sample ID BHV-5 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 1.11 752 2110 18 5.5 244 3.0 0.4 442 44 2.2 MOC -Minimum detectable concentration Units mglfilter pCilFilter pC ilFi Iter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter pC ilFi Iter pCilFilter pCilFilter Qualifiers Rl 0.0003 0.2 Report Date: 05/27/12 Collection Date: 04/03/12 DateReceived: 04/06/12 Matrix: Filter MCU QCl Method Analysis Date 1 By SW6020 04/11/1220:351 cp SW6020 04/11/1220:351 cp E909.0 04/28/12 08:241 eli-cs E909.0 04/28/12 08:241 eli-cs E909.0 04/28/12 08:241 eli-cs E903.0 05/15/12 12:43 1 trs E903.0 05/15/12 12:43 1 trs E903.0 05/15/12 12:431 trs E908.0 04/17/12 17:241 dmf E908.0 04/17/12 17:241 dmf E908.0 04/17/12 17:241 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 22 EN:RGY LABORATORIES www.energylab.com Anatrtica/ Excellence Since 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 27, 2012 PROJECT: lst Quarter Air 2012 SAMPLE ID: BHV-6 QuarterlDate Sampled Radionuclide Concentration Air Volume JlCilmL C 12040316-005 natu 4.41E-15 First Quarter 2012 230Th 1.82E-15 Air Volume in mLs 226Ra 4.00E-16 1.36E+ll 210pb 1.50E-14 +LLD's are from Reg. Guide 4.14 Counting Precision JlCilmL N/A 2E-16 lE-17 lE-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCJlCilmL N/A 2E-17 3E-18 4E-17 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration lE-16 9E-14 4.90E+00 lE-16 3E-14 6.08E+00 lE-16 9E-13 4.45E-02 2E-15 6E-13 2.50E+00 Page 11 of 22 EN:RGY LABORATORIES www.energylab.com ~Helena.MTB77-472-0711 .Billings.MT 800-135-4489 . Casper, WY 888-235-0515 AnalyticalfxcsllsnCBSiI1C8 7852 J " . Gillette, WY 86&-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 1 st Quarter Air 2012 Lab ID: C 1204031 6-005 Client Sample ID BHV-6 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.887 601 2040 17 5.4 54.6 1.3 0.4 248 26 2.3 MOC -Minimum detectable concentration Units mg/filter pCilFilter pCilFilter pC ilFi Iter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter pC ilFi Iter Qualifiers Rl 0.0003 0.2 Report Date: OS/27/12 Collection Date: 04/03/12 DateReceived: 04/06/12 Matrix: Filter MCL! QCl Method Analysis Date 1 By SW6020 04/11/12 07:561 smm SW6020 04/11/1207:561 smm E909.0 04/28/12 10:391 eli-cs E909.0 04/28/12 10:391 eli-cs E909.0 04/28/12 10:391 eli-cs E903.0 05/15/12 12:431 trs E903.0 05/15/12 12:431 trs E903.0 05/15/12 12:43 1 trs E908.0 04/17/1217:24/dmf E908.0 04/17/12 17:24/ dmf E908.0 04/17/1217:241 dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 12 of 22 EN:RGY L ABORATORIES www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: May 27, 2012 PROJECT: 1st Quarter Air 2012 SAMPLE ID: Blank/2A QuarterlDate Sampled Radionuclide Concentration Air Volume pCilmL C 12040316-006 natU 1.37E-17 First Quarter 2012 230Th 5.82E-18 Air Volume in mLs 226Ra 7.24E-18 1.36E+ll 210Pb -5.71E-18 Counting Precision pCilmL N/A 2E-18 2E-18 2E-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCpCilmL N/A 2E-18 3E-18 4E-17 L.L.D.+ Effluent Cone. * % Effluent pCilmL pCilmL Concentration lE-16 9E-14 1.52E-02 lE-16 3E-14 1.94E-02 lE-16 9E-13 8.04E-04 2E-15 6E-13 -9.52E-04 Page 13 of 22 EN:RGY LABORATORIES www.energylab.com Analytical fxcsllsncB SiI1C8 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-686-1175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 1 st Quarter Air 2012 Lab ID: C 1204031 6-006 Client Sample ID Biankl2A Analyses TRACE METALS- Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.0028 1.9 -0.8 3.2 5.4 1 0.3 0.4 0.79 0.27 0.21 MOC -Minimum detectable concentration Units mg/fifter pC ilFi Iter pCilFilter pC ilFi Iter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter pCilFilter Report Date: 05/27/12 Collection Date: 04/03/12 DateReceived: 04/06/12 Matrix: Filter MCU Qualifiers Rl QCl Method Analysis Date 1 By 0.0003 SW6020 04/11/12 20:37 1 cp 0.2 SW6020 04/11/1220:371 cp U E909.0 04/28/12 12:53 1 eli-cs E909.0 04/28/12 12:53 1 eli-cs E909.0 04/28/12 12:53 1 eli-cs E903.0 05/15/12 12:431 trs E903.0 05/15/12 12:431 trs E903.0 05/15/12 12:43 1 trs E908.0 04/17/1217:241 dmf E908.0 04/17/1217:241 dmf E908.0 04/17/1217:24/dmf MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 14 of 22 EN:RGY LABORATORIES --------m.11 www.energylab.com ~~ Analytical Exes/Isncs SinclI 7952 [--- Helena, MT 877 ~4 72-0711 • Billings, MT 800-735-4489 • Casper, WV 888-235-0515 .... ' Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, lX 888-690-2218 Client: Denison Mines USA Corp Project: 1 st Quarter Air 2012 QA/QC Summary Report Prepared by Casper, WY Branch Report Date: OS/27/12 Work Order: C12040316 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E903.0 Sample 10: C12040240-009AMS Radium 226 Sample 10: C12040240-009AMSO Radium 226 Sample 10: LCS-33282 Radium 226 Sample 10: MB-33282 Radium 226 Radium 226 precision (±) Radium 226 MDC Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration Sample Matrix Spike 127 pCi/Filter Sample Matrix Spike Duplicate 133 pCi/Filter Laboratory Control Sample 12.5 pCi/Filter Method Blank 0.1 pCi/Filter 0.05 pCi/Filter 0.07 pCi/Filter Batch: 33282 Run: G542M_12041 OA 05/15/12 00:23 107 70 130 Run: G542M_120410A 05/15/12 00:23 106 70 130 4.8 14.7 Run: G542M_12041 OA 05/15/12 12:43 103 70 130 Run: G542M_120410A 05/15/12 12:43 ND -Not detected at the reporting limit. Page 15 of 22 EI\ERGY LABORATORIES www.energyJab.com Aoalytical [xutlsncdines rg52 Helena, MT 877 -412-0711 . Billings, MT 800-735-4489 • Casper, WV888-235-0515 Gillette, WY 866-&86-7115 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1 st Quarter Air 2012 Analyte Count Result Units Method: E908.0 Sample 10: C12040240-003AMS Thorium 230 Sample 10: C12040240-003AMSO Thorium 230 Sample 10: LCS-33282 Thorium 230 Sample 10: MB-33282 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Qualifiers: RL -Analyte reporting limit. Sample Matrix Spike 51.0 pCi/Filter Sample Matrix Spike Duplicate 53.5 pCi/Filter Laboratory Control Sample 10.1 pCi/Filter 3 Method Blank 0.1 pCi/Filter 0.08 pCilFilter 0.1 pCi/Filter MDC -Minimum detectable concentration Report Date: OS/27/12 Work Order: C12040316 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: ALPHANAL YST _120413A 99 70 130 Run: ALPHANALYST_120413A 104 70 130 4.8 Run: ALPHANAL YST _120413A 102 80 120 Run: ALPHANAL YST _120413A ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: R158737 04/17/12 17:23 04117/1217:23 30.6 04/17/12 17:24 04/17/1217:24 U Page 16 of 22 EN:RGY L A BORATORIES .. _---tlQ" www.energylab.com J.; Analytical Exes/Isnce Sincs 1952 Helena, MT 877~472-0711 • Billings, M:T 800~135~4489 • Casper, WY888-235-0515 Gillette, WY 86&-686-7175 • Rapid City, SD 888-612-1225 • College Station, IX 888-690-2218 Client: Denison Mines USA Corp Project: 1 st Quarter Air 2012 QA/QC Summary Report Prepared by Casper, WY Branch Report Date: OS/27/12 Work Order: C12040316 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E909.0 Sample 10: MB-16115 Lead 210 Lead 210 precision (±) Lead 210 MDC Sample 10: LCS-16115 Lead 210 Sample 10: T12040068-001 AMS Lead 210 Sample 10: T12040068-001AMSO Lead 210 Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration Method Blank -0.2 pCi/Filter 3 pCi/Filter 5 pCi/Filter Laboratory Control Sample 495 pCi/Filter Sample Matrix Spike 1710 pCi/Filter Sample Matrix Spike Duplicate 1690 pCi/Filter Run: SUB-T45199 Run: SUB-T45199 94 70 130 Run: SUB-T45199 104 70 130 Run: SUB-T45199 102 70 130 NO -Not detected at the reporting limit. 1.4 Batch: T _16115 04/26/12 15:58 U 04/26/12 18:12 04/26/12 22:42 04/27/1200:57 13.5 U -Not detected at minimum detectable concentration Page 17 of 22 EN:RGY LABORATORIES ~ .. ",,,, ~ Client: Denison Mines USA Corp Project: 1 st Quarter Air 2012 Helena, MT 877 .. 472-0711 • Billings,. MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-&86-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Report Date: OS/27/12 Work Order: C12040316 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW6020 Sample 10: ICV Uranium Method: SW6020 Sample 10: MB-33282 Uranium Sample 10: LCS2-33282 Uranium Sample 10: C12040240-002AOIL Uranium Sample 10: C12040316-006AMS Uranium Sample 10: C12040316-006AMSO Uranium Method: SW6020 Sample 10: ICV Uranium Method: SW6020 Sample 10: MB-33282 Uranium Sample 10: LCS2-33282 Uranium Sample 10: C12040240-001 AOIL Uranium Sample 10: C12040316-006AMS Uranium Sample 10: C12040316-006AMSO Uranium Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Analytical Run: ICPMS2-C _120411 B Initial Calibration Verification Standard 04/11/1205:05 0.0494 mg/L 0.00030 99 90 110 Batch: 33282 Method Blank Run: ICPMS2-C_120411 B 04/11/1207:12 ND mg/filter 6E-05 Laboratory Control Sample Run: ICPMS2-C_120411 B 04/11/1207:14 0.104 mg/filter 0.00030 104 85 115 Serial Dilution Run: ICPMS2-C _120411 B 04/11/1207:25 0.00776 mg/filter 0.0014 6.9 20 Sample Matrix Spike Run: ICPMS2-C_120411 B 04/11/12 07:59 0.0488 m g/fi Iter 0.00030 93 75 125 Sample Matrix Spike Duplicate Run: ICPMS2-C_120411 B 04/11/1208:01 0.0492 mg/filter 0.00030 94 75 125 0.8 20 Analytical Run: ICPMS2-C _120411 C Initial Calibration Verification Standard 04/11/1214:51 0.0494 mg/L Method Blank ND mg/filter Laboratory Control Sample 0.101 mg/filter Serial Dilution 0.000451 mg/filter Sample Matrix Spike 0.0509 mg/filter Sample Matrix Spike Duplicate 0.0515 mg/filter 0.00030 99 90 110 Batch: 33282 Run: ICPMS2-C_120411C 04/11/1220:07 6E-05 Run: ICPMS2-C_120411C 04/11/12 20:09 0.00030 101 85 115 Run: ICPMS2-C_120411C 04/11/1220:14 0.0014 20 N Run: ICPMS2-C_120411C 04/11/12 20:39 0.00030 96 75 125 Run: ICPMS2-C_120411C 04/11/1220:40 0.00030 97 75 125 1.0 20 ND -Not detected at the reporting limit. N -The analyte concentration was not sufficiently high to calculate a RPD for the serial dilution test. Page 18 of 22 EN:RGY LAE30RAT ORI ES -----===t=~=ett . www ..... gji.t>com ~.H.lena.MT 811-412"0111 • Blillng~ MT 800-135-4489 • Casper, WI 888"235-0515 . ~ ~~-AnaIyticaI~tlsm;flSinCB 1952 J;c;/t·:~ .. GiUette, WY 866-686-7175 . Rapid C~ty, SO 888-672-1225 . College Station, lX 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp Login completed by: Kristy Gisse Reviewed by: BL2000\kschroeder Reviewed Date: 4/12/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Container/Temp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 ' Yes 0 Yes 0 N/A'C NA Yes D Yes D III~I illllll~11 ~I~ IIIII~ 1I111111111 C12040316 Date Received: 4/6/2012 Received by: kg Carrier NDA name: No D No D No D No D No D No D No D No D No D No D No D No D Not Present D Not Present D Not Present 0 No VOA vials submitted 0 Not Applicable 0 Page 19 of 22 "U Q) , co CD I\J o o -I\J I\J Chain of Custody and Analytical Request Record Page .-L-of _,_ IU.(~"Y "fR.j~ll!il.iNhi. PLEASE PRINT (Provide as much information as possible.) Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: De('\\.son M~"e:5> 1 >-r ~··h~r A: r 20';2.. State: \AT Yes !Xl No 0 Report Mail Address: Po BC)< ~O'i Contact Name: Phone/Fax: Email: Sampler: (Please Print) t31M~~~C\ ~ ~45H &~'("r~" ?~\mef' y~ 67g ~I &QJ'r"1\ l:~If'1er Invoice Address: ~ Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: .s~rY)e-D~"\l ~~ -rv-.r~ "1:5..& '7K ;txt l Special Report/Formats: 3: &lRl&I1W~O~ OO~®(ID[g@lJ~[ID • Contact ELI prior to . ~StliIPPiCJbY: 1ft\. A o "-RUSH sample submittal ' I "4-. I,J \ iA ~ 0 V) ~ _ for charges and ~,..mD(S~ ~ Ill;g 01 2 0 ~ R scheduling -See 1ix } ,-> 0 >. ('0 I-.. ) O DW 0 EDD/EDT . ~(/)~ ~ S LU -Instruction Page (Electronic Data) o::;:....!2 V) ........ I 'U R I T O ::>·0 ('0 ....,. , '\ s::: Ct· ace tt emp POTWIWWTP Format: U «(/)1.2 ~ ~ ::l U ommen s. l-e,;1\ o State' 0 LEVEL IV ~ <D2~1.§ ~ ~ 2f' ,," ~ '" tJ B. 0 C D · D ~ c.. co.2 C1 I-E lv _ .... ~ 1-========-=--1 Other: NELAC E ~119 · 0 . ft « ::l \~ ""\t'{V""'-.J On tce: Y N ~ CJ.).-CJ.) $: 1"': '-JI Q I-5 (;0 \?-z c. <I ~o 6 t1 N _ W "E ,1').0 Custody Seal ~ >1 '""'\ ("( r{ ci LU {g '\ \ ~ ()-On Bottle .:L N (/) <. 1 f C/) &i I ( ,.0 On Cooler W N ~ _________ ~ ___ ~ ___ ~ __ ~1~~' ~ H ~3 ~ ~N SAMPLE IDENTIFICATION Collection Collection MATRIX ~ "a-rJ ;:fJ, Signature (Name, Location, Interval, etc.) Date Time ~ ~ Match N 1 f,i4 V -) i /:3/:JJl \ ':l.. '1b1~... 1 ::, -A 'f:. 'f-',( 'I. I~ 2 ~H\J-:l.. lil:3~l~ '(. 'f. X ~ ~ 3 BH\)-Y ~ 'f.. 'l'f.. ~ 413~\J_ 5 11-. ~~ 1)(. ~ 5 B\hJ _ ~ \)( "--'f.. ~ I~ 6 ~\G..n\(./ 2.A l/3J:lD1'2..-HI3/rJ 1 ~. -A Y. Y. 'f ~ ~ 7 1.\ 1~'2..· ~(.11-b ~3l <-- 8 ~ 9 I~ I~ \ 10 ~ Custody .. ~~U~;by~:nltl~A'" ~J~i~ I'M 41"IfJJtJ);i91!JLL-'1 Received by (print): Daternme: Signature: Record Relinquished by (print): \] Daternme: '-' Signature: '-...../ Received by (print): OatefTime: Signature: MUST be I • 1(4M:Glvea by Laooratory: I~e!llme: -.::.:.-1,,. -SIgn Jure: I Signed Sample Disposal: Return to Client Lab Disposal: LI .... lo-~'"' q:\S ~MlW: 'JAi'}.,fh'/ This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. plete the an~ req~ed, Visit our web site at www.energylab,com for additional information, downloadable fee schedule, forms, and links. www.energylab.com EI\ERGY LABORATORIES Analytical ExcsJIBf/CB Sines 1952 Helena, MT 877-412-071 t • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 'Gillett~J WY .866 .. 686-7115 • Rapid City, SO 888-&72-1225 • College Station, IX 888-690-2218 ANALYTICAL SUMMARY REPORT August 10, 2012 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C 12070341 Project Name: 2nd Quarter Air 2012 Energy Laboratories, Inc. Casper WY received the following 6 samples for Denison Mines USA Corp on 7/11/2012 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C12070341-001 BVH-1 07/02/1200:0007/11/12 Filter Composite of two or more samples Metals, Total Digestion, Total Metals Lead 210 Radium 226 Thorium, Isotopic C 12070341-002 BHV-2 07/02/12 00:00 07/11/12 Filter Same As Above C 12070341-003 BHV-4 07/02/1200:0007/11/12 Filter Same As Above C 12070341-004 BHV-5 07/02/1200:00 07/11/12 Filter Same As Above C 12070341-005 BVH-6 07/02/12 00:00 07/11/12 Filter Same As Above C12070341-006 Blank 07/02/1200:00 07/11/12 Filter Same As Above The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: Digitally signed by Steve Carlston Date: 2012.08.10 17:27:56 -06:00 Page 1 of 22 www.energyJab.com Analytical Exf;BHtHlCB Sines 1952 Helena, MT 877 .. 472-0111 • Billings, MT 800-735-4489 • Casper, WY 888~235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 CLIENT: Denison Mines USA Corp Project: 2nd Quarter Air 2012 Report Date: 08/10/12 Sample Delivery Group: C12070341 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the ch illing process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewe9 as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001 , Radiochemical WY200002; Utah: WY00002; Virginia: 00057; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. Page 2 of 22 EI\ERGY LABORATORIES www.energylab.com Ana/ftical Excellence Since 1952 Helena, MT 817-472-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 10, 2012 PROJECT: 2nd Quarter Air 2012 SAMPLE ID: BVH-1 QuarterlDate Sampled Radionuclide Concentration Air Volume fJCilmL C 12040316-00 1 natU 7.87E-16 First Quarter 2012 230Th 2.64E-16 Air Volume in mLs 226Ra 3.95E-16 1.37E+ 11 210Pb 1.25E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume fJCilmL C12070341-001 natU 1.86E-15 Second Quarter 2012 230Th 8.33E-16 Air Volume in mLs 226Ra 9.85E-16 1.33E+11 210Pb 9.55E-15 +LLD's are from Reg. Guide 4.14 Counting Precision fJCilmL N/A 3E-17 1E-17 1E-16 Counting Precision fJCilmL N/A 9E-17 5E-17 2E-16 *Effluent Concentration from the NEW 10 CFR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCfJCilmL N/A 6E-18 3E-18 4E-17 MDCfJCilmL N/A 7E-18 9E-18 6E-17 L.L.D.+ Effluent Cone. * % Effluent fJCilmL fJCilmL Concentration 1E-16 9E-14 8.75E-01 1E-16 3E-14 8.80E-01 1E-16 9E-13 4.39E-02 2E-15 6E-13 2.08E+00 L.L.D.+ Effluent Cone. * % Effluent fJCilmL fJCilmL Concentration 1E-16 9E-14 2.06E+00 1E-16 3E-14 2.78E+00 1E-16 9E-13 1.09E-01 2E-15 6E-13 1.59E+00 Page 3 of 22 EN:RGY LABORATORIES www.energylab.com Analytical ucslJ8flCfI SiIlCB 71152 Helena, MT 877-472-0711 .' Billings, MT 800-735-4489 11 Casper, WY 888-235-0515 Gillette, WY .866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 2nd Quarter Air 2012 C12070341-001 Client Sample ID BVH-1 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MDC Radium 226 Radium 226 precision (±) Radium 226 MDC Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.366 248 1270 26 8.3 131 6.4 1.2 111 12 1.0 MDC -Minimum detectable concentration Units mgifilter pC ilFi Iter pCilFilter pC ilFi Iter pC ilFi Iter pC ilFi Iter pCi/Filter pC ilFi Iter pC ilFi Iter pC ilFi Iter pCilFilter Report Date: 08/10/12 Collection Date: 07/02/12 DateReceived: 07/11/12 Matrix: Filter MCL! Qualifiers Rl QCl Method Analysis Date / By D D 0.003 SW6020 2 SW6020 E909.0 E909.0 E909.0 E903.0 E903.0 E903.0 E908.0 E908.0 E908.0 MCl -Maximum contaminant level. ND -Not detected at the reporting limit. D -Rl increased due to sample matrix. 08/04/12 18:03 1 cp 08/04/12 18:03 1 cp 07/31/1209:231 eli-cs 07/31/1209:231 eli-cs 07/31/1209:231 eli-cs 07/24/1200:041 trs 07/24/1200:041 trs 07/24/1200:041 trs 07/25/12 11 :39 1 dmf 07/25/12 11 :39 1 dmf 07/25/12 11 :39 1 dmf Page 4 of 22 EN:RGY LABORATORIES www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-472-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 10,2012 PROJECT: 2nd Quarter Air 2012 SAMPLE ID: BHV-2 QuarterlDate Sampled Radionuclide Concentration Air Volume IlCilmL C 12040316-002 natU 4.22E-16 First Quarter 2012 230Th 1.15E-16 Air Volume in mLs 226Ra 2.77E-16 1.37E+ll 210Pb 1.58E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume IlCilmL C12070341-002 natU 3.39E-16 Second Quarter 2012 230Th 1.56E-16 Air Volume in mLs 226Ra 1.74E-16 1.34E+ll 210Pb 8.60E-15 +LLD's are from Reg. Guide 4.14 Counting Precision IlCilmL N/A 2E-17 9E-18 1E-16 Counting Precision IlCilmL N/A 2E-17 2E-17 2E-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCIlCilmL N/A 4E-18 3E-18 4E-17 MDC IlCilmL N/A 5E-18 9E-18 6E-17 L.L.D.+ Effluent Cone. * % Effluent IlCilmL IlCilmL Concentration 1E-16 9E-14 4.68E-Ol lE-16 3E-14 3.84E-Ol lE-16 9E-13 3.07E-02 2E-15 6E-13 2.63E+00 L.L.D.+ Effluent Cone. * % Effluent IlCilmL IlCilmL Concentration lE-16 9E-14 3.76E-01 lE-16 3E-14 5.19E-Ol lE-16 9E-13 1. 94E-02 2E-15 6E-13 1.43E+00 Page 5 of 22 EN:RGY LABORATORIES www.energylab.com Analytical Excel/BfleB Sines 7952 Helena, MT 877-412-0711 • Billings, MT 800-735-4489 . Casper, WV 888-235-0515 Gillette, WY.866-686-7175 • Rapid City, SI} 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 2nd Quarter Air 2012 Lab ID: C 12070341-002 Client Sample ID BHV-2 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.067 46 1160 25 8.4 23.4 2.7 1.2 21 2.7 0.65 MOC -Minimum detectable concentration Units mgifilter pCilFilter pCilFilter pCilFilter pC ilFi Iter pC ilFi Iter pC ilFi Iter pC ilFi Iter pC ilFi Iter pC i/Fi Iter pC ilFi Iter Report Date: 08/10/12 Collection Date: 07/02/12 DateReceived: 07/11/12 Matrix: Filter MCL! Qualifiers Rl QCl Method Analysis Date 1 By 0 0 0.003 SW6020 2 SW6020 E909.0 E909.0 E909.0 E903.0 E903.0 E903.0 E908.0 E908.0 E908.0 MCl -Maximum contaminant level. NO -Not detected at the reporting limit. 0-Rl increased due to sample matrix. 08/04/12 18:39 1 cp 08/04/12 18:39 1 cp 07/31/12 17:441 eli-cs 07/31/12 17:441 eli-cs 07/31/12 17:441 eli-cs 07/24/1200:041 trs 07/24/12 00:04 1 trs 07/24/12 00:04 1 trs 07/25/12 11 :39 1 dmf 07/25/12 11 :39 1 dmf 07/25/12 11 :39 1 dmf Page 6 of 22 www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 (lillette, WY 866-686-7175 • Rapid City, SD 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 10,2012 PROJECT: 2nd Quarter Air 2012 SAMPLE ID: BHV-4 QuarterlDate Sampled Radionuclide Concentration Air Volume JlCilmL C12040316-003 natu 2.51E-15 First Quarter 2012 230Th 5.02E-16 Air Volume in mLs 226Ra 2.27E-16 1.36E+11 210Pb 1.03E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C12070341-003 natU 2.62E-15 Second Quarter 2012 230Th 1.23E-15 Air Volume in mLs 226Ra 2.97E-16 1.35E+l1 210Pb 9.27E-15 +LLD's are from Reg. Guide 4.14 Counting Precision JlCilmL N/A 6E-17 8E-18 1E-16 Counting Precision JlCilmL N/A 1E-16 3E-17 2E-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCJlCilmL N/A 9E-18 3E-18 4E-17 MDC JlCilmL N/A 6E-18 9E-18 6E-17 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration 1E-16 9E-14 2.79E+00 1E-16 3E-14 1.67E+00 1E-16 9E-13 2.52E-02 2E-15 6E-13 1. 72E+OO L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration lE-16 9E-14 2.91E+00 lE-16 3E-14 4.lOE+00 lE-16 9E-13 3.30E-02 2E-15 6E-13 1.55E+00 Page 7 of 22 EN:RGY LABORATORIES www.energylab.com Analytit:JIl Exesllence Sines 1952 , ' Helena, MT 877-472-0711 • Billings, MT 800-735-4489 " Casper, WY 888-235-0515 Gillette,WY866 .. &B6-7175 • Rapid City, SD 888-672-1225 • College station, IX 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 2nd Quarter Air 2012 Lab ID: C 12070341 -003 Client Sample ID BHV-4 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCL -Quality control limit. Result 0.522 354 1250 25 8.3 40.1 3.7 1.3 166 16 0.87 MOC -Minimum detectable concentration Units mgifilter pC ilFi Iter pC ilFi Iter pC ilFi Iter pC ilFi Iter pCilFilter pCi/Filter pC ilFi Iter pC ilFi Iter pC i/Fi Iter pCi/Filter Report Date: 08/10/12 Collection Date: 07/02/12 DateReceived: 07/11/12 Matrix: Filter MCL! Qualifiers Rl QCl Method Analysis Date 1 By 0 0 0.003 SW6020 2 SW6020 E909.0 E909.0 E909.0 E903.0 E903.0 E903.0 E908.0 E908.0 E908.0 MCl -Maximum contaminant level. NO -Not detected at the reporting limit. o -RL increased due to sample matrix. 08/04/12 18:431 cp 08/04/12 18:43 1 cp 07/31/12 12:081 eli-cs 07/31/12 12:08 1 eli-cs 07/31/1212:081 eli-cs 07/24/1200:04/trs 07/24/12 00:04 1 trs 07/24/1200:041 trs 07/25/12 11 :39 1 dmf 07125/12 11 :39 1 dmf 07125/12 11 :39 1 dmf Page 8 of 22 EN:RGY L ABORATORIES www.energylab.com Ana/Tfical Excellence Since 1952 Helena, MT 877-412-0111 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 Gillette, WY 86&-686-7115 • Rapid City, SD 888-612-1225 • College Station, TX 888-&90-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 10,2012 PROJECT: 2nd Quarter Air 2012 SAMPLE ID: BHV-5 QuarterlDate Sampled Radionuclide Concentration Air Volume JlCilmL C 12040316-004 nalU 5.52E-15 First Quarter 2012 230Th 3.24E-15 Air Volume in mLs 226Ra 1.79E-15 1.36E+ll 210Pb 1.55E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume JlCilmL C12070341-004 natU 5.87E-15 Second Quarter 2012 230Th 3.06E-15 Air Volume in mLs 226Ra 1.21E-15 1.22E+l1 210Pb 1. llE-14 +LLD's are from Reg. Guide 4.14 Counting Precision JlCilmL N/A 3E-16 2E-17 lE-16 Counting Precision JlCilmL N/A 3E-16 6E-17 2E-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDC JlCilmL N/A 2E-17 3E-18 4E-17 MDC JlCilmL N/A 2E-17 lE-17 7E-17 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration lE-16 9E-14 6. 13E+OO lE-16 3E-14 1.08E+Ol lE-16 9E-13 1.99E-01 2E-15 6E-13 2.58E+00 L.L.D.+ Effluent Cone. * % Effluent JlCilmL JlCilmL Concentration lE-16 9E-14 6.52E+00 lE-16 3E-14 1.02E+Ol lE-16 9E-13 1.35E-OI 2E-15 6E-13 1. 85E+00 Page 9 of 22 EN:RGY LABORATORIES www.energylab.com Analytical ExcsJlsnCB Sines 1952 Helena, MT B77~412-0711 • Billings, MT 800-735~4489 • Casper, WY 888-235~0515 Giliette, WY866~6B6~1175 • Rapid City, SD 888-672 .. 1225 • College Station, IX 888-690~2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 2nd Quarter Air 2012 C12070341-004 Client Sample ID BHV-5 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES Lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 1.06 715 1350 26 8.3 148 6.9 1.3 373 35 2.2 MOC -Minimum detectable concentration Units mg/filter pC ilFi Iter pC ilFi Iter pC ilFi Iter pC ilFi Iter pCi/Filter pC ilFi Iter pCilFilter pC ilFi Iter pC ilFi Iter pC ilFi Iter Report Date: 08/10/12 Collection Date: 07/02/12 DateReceived: 07/11/12 Matrix: Filter MCL! Qualifiers RL QCL Method Analysis Date / By 0 0 0.003 SW6020 2 SW6020 E909.0 E909.0 E909.0 E903.0 E903.0 E903.0 E908.0 E908.0 E908.0 MCl -Maximum contaminant level. NO -Not detected at the reporting limit. 0-Rl increased due to sample matrix. 08/04/12 18:48 1 cp 08/04/12 18:48 1 cp 07/31/1218:31 1 eli-cs 07/31/1218:31 1 eli-cs 07/31/1218:31 1 eli-cs 07/24/12 00:041 trs 07/24/1200:041 trs 07/24/1200:041 trs 07/25/12 11 :39 1 dmf 07/25/1211 :39 1 dmf 07/25/12 11 :39 1 dmf Page 10 of 22 EN:RGY LABORATORIES www.energylab.com Ans/rficsJ Excellence Since 1952 Helena, MT 877-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7115 • Rapid City, SD 888-612-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 10, 2012 PROJECT: 2nd Quarter Air 2012 SAMPLE ID: BVH-6 QuarterlDate Sampled Radionuclide Concentration Air Volume fJCilmL C12040316-005 natU 4.41E-15 First Quarter 2012 230Th 1.82E-15 Air Volume in mLs 226Ra 4.00E-16 1. 36E+ 11 2IOPb 1.50E-14 QuarterlDate Sampled Concentration Radionuclide Air Volume fJCilmL C12070341-005 natu 6.42E-15 Second Quarter 2012 230Th 2.25E-15 Air Volume in mLs 226Ra 5.11E-16 1.26E+ll 2IOPb 9.54E-15 +LLD's are from Reg. Guide 4.14 Counting Precision fJCilmL N/A 2E-16 lE-17 lE-16 Counting Precision fJCilmL N/A 2E-16 4E-17 2E-16 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCfJCilmL N/A 2E-17 3E-18 4E-17 MDC fJCilmL N/A lE-17 lE-17 7E-17 L.L.D.+ Effluent Cone. * % Effluent fJCilmL fJCilmL Concentration lE-16 9E-14 4.90E+00 lE-16 3E-14 6.08E+00 lE-16 9E-13 4.45E-02 2E-15 6E-13 2.50E+00 L.L.D.+ Effluent Cone. * % Effluent fJCilmL fJCilmL Concentration lE-16 9E-14 7.13E+00 lE-16 3E-14 7.50E+00 lE-16 9E-13 5.67E-02 2E-15 6E-13 1.59E+00 Page 11 of 22 EN:RGY LABORAT ORIES WWN.energylab.com Analytical Excellence Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 'Giliefte, WY 866-686-7175 • Rapid City, so 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 2nd Quarter Air 2012 Lab 10: C 12070341-005 Client Sample 10 BVH-6 Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 1.19 BOB 1200 25 B.3 64.2 4.6 1.3 2B3 27 1.6 MOC -Minimum detectable concentration Units mg/filter pC ilFi Iter pCilFilter pC ilFi Iter pC ilFi Iter pCilFilter pC ilFi Iter pC ilFi Iter pC ilFi Iter pCilFilter pCilFilter Report Date: 08/10/12 Collection Date: 07/02/12 DateReceived: 07/11/12 Matrix: Filter MCL! Qualifiers Rl QCl Method Analysis Date / By 0 0 0.003 SW6020 2 SW6020 E909.0 E909.0 E909.0 E903.0 E903.0 E903.0 E90B.0 E90B.0 E90B.0 MCl -Maximum contaminant level. NO -Not detected at the reporting limit. 0 -Rl increased due to sample matrix. OBI04/12 1B:52 1 cp OBI04/12 1B:52 1 cp 07/31/12 12:561 eli-cs 07/31/1212:561 eli-cs 07/31/1212:561 eli-cs 07/24/12 00:04 1 trs 07/24/1200:041 trs 07/24/1200:041 trs 07/25/12 11 :39 1 dmf 07/25/1211 :39 1 dmf 07/25/12 11 :39 1 dmf Page 12 of 22 www.energylab.com Analytical Excellence Since 1952 Helena, MT 877-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SO 888-672-1225 • College Station, TX 888-690-2218 HIGH VOLUME AIR SAMPLING REPORT CLIENT: Denison Mines USA Corp REPORT DATE: August 10, 2012 PROJECT: 2nd Quarter Air 2012 SAMPLE ID: Blank QuarterlDate Sampled Radionuclide Concentration Air Volume plCilmL C12040316-006 natU 1.37E-17 First Quarter 2012 230Th 5.82E-18 Air Volume in mLs 226Ra 7.24E-18 1.36E+11 210Pb -5.71E-18 Counting Precision plCilmL N/A 2E-18 2E-18 2E-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. QuarterlDate Sampled Concentration Counting Radionuclide Precision Air Volume plCilmL plCilmL C 12070341-006 natu 2.08E-17 N/A Second Quarter 2012 230Th 7.76E-18 2E-18 Air Volume in mLs 226Ra 2.00E-18 5E-18 1.36E+11 210Pb 1.82E-17 4E-17 Note: This sample uses 136,000,000 L of air volume for comparison purposes. +LLD's are from Reg. Guide 4.14 *Effluent Concentration from the NEW 10 CPR Part 20 -Appendix B -Table 2 Year for Natural Uranium Year for Thorium-230 Week for Radium-226 Day for Lead-21O MDCplCilmL N/A 2E-18 3E-18 4E-17 MDC plCilmL N/A 2E-18 9E-18 7E-17 L.L.D.+ Effluent Cone. * % Effluent plCilmL plCilmL Concentration 1E-16 9E-14 1.52E-02 1E-16 3E-14 1.94E-02 1E-16 9E-13 8.04E-04 2E-15 6E-13 -9.52E-04 L.L.D.+ Effluent Cone. * % Effluent plCilmL plCilmL Concentration 1E-16 9E-14 2.31E-02 1E-16 3E-14 2.59E-02 1E-16 9E-13 2.22E-04 2E-15 6E-13 3.04E-03 Page 13 of 22 EI\ERGY LABORATORIES ~.-.. -.,.,,,, ~ WWN.energylab.com Analytical ExcsJISflCB Sines 1952 Helena, MT 877 -472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 GillettQ, WY866-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Denison Mines USA Corp 2nd Quarter Air 2012 LablD: C 12070341-006 Client Sample ID Blank Analyses TRACE METALS Uranium Uranium, Activity RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC Radium 226 Radium 226 precision (±) Radium 226 MOC Thorium 230 Thorium 230 precision (±) Thorium 230 MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 0.004 3 2.5 5.7 9.5 0.3 0.7 1.2 1.1 0.33 0.22 MOC -Minimum detectable concentration Units mgifilter pC ilFi Iter pC ilFi Iter pCilFilter pCilFilter pCilFilter pCilFilter pC i/Fi Iter pC ilFi Iter pC ilFi Iter pCi/Filter U -Not detected at minimum detectable concentration Report Date: 08/10/12 Collection Date: 07/02/12 DateReceived: 07/11/12 Matrix: Filter MCL! Qualifiers Rl QCl Method Analysis Date 1 By 0 0 U U 0.003 SW6020 2 SW6020 E909.0 E909.0 E909.0 E903.0 E903.0 E903.0 E908.0 E908.0 E908.0 MCl -Maximum contaminant level. NO -Not detected at the reporting limit. o -R l increased due to sample matrix. 08/04/12 18:57 1 cp 08/04/12 18:57 1 cp 07/31/1213:441 eli-cs 07/31/1213:441 eli-cs 07/31/12 13:44 1 eli-cs 07/24/1201 :49 1 trs 07/24/1201 :49 1 trs 07/24/1201 :49 1 trs 07/25/12 11 :39 1 dmf 07/25/12 11 :39 1 dmf 07125/12 11 :39 1 dmf Page 14 of 22 EN:RGY www.energylab.com Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 .Gillefte, WY 8&6-686-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORIES Analytical ExCBIISflCB Sines 1952 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 2nd Quarter Air 2012 Analyte Count Result Units Method: E903.0 Sample 10: MB-34300 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: LCS-34300 Radium 226 Sample 10: C12070341 -001AMS Radium 226 Sample 10: C12070341-001AMSO Radium 226 Qualifiers: RL -Analyte reporting limit. 3 MDC -Minimum detectable concentration Method Blank -0.2 pCi/Filter 0.1 pCi/Filter 0.3 pCi/Filter Laboratory Control Sample 11 .5 pCi/Filter Sample Matrix Spike 226 pCi/Filter Sample Matrix Spike Duplicate 249 pCi/Filter Report Date: 08/10/12 Work Order: C12070341 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: BERTHOLD 770-2_120716A Run: BERTHOLD 770-2_120716A 98 70 130 Run: BERTHOLD 770-2_120716A 79 70 130 Run: BERTHOLD 770-2_120716A 101 70 130 9.8 ND -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Batch: 34300 07/24/1200:04 U 07/24/1200:04 07/24/1200:04 07/24/1200:04 20.5 Page 15 of 22 EN:RGY LABORATORIES www.energylab.com Analytical ExcsJIBflCB SiIlCB 1952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ~ilJett~, WY866 .. 686~7175 .. Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 2nd Quarter Air 2012 Analyte Count Method: E908.0 Result Units Sample 10: C12070088-008AOUP Thorium 230 3 Sample Duplicate Thorium 230 precision (±) Thorium 230 MDC 0.8 pCi/Filter 0.4 pCi/Filter 0.4 pCi/Filter Report Date: 08/10/12 Work Order: C12070341 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: ALPHANAL YST _120723A 81 Batch: R 162569 07/25/12 11 :39 111 .7 -Sample was not spiked and is reported as a Duplicate. All tracer recoveries are acceptable therefore the batch is approved. Sample 10: C12070088-008AOUP Thorium 230 Thorium 230 precision (±) Thorium 230 MDC 3 Sample Duplicate 0.7 pCi/Filter 0.4 pCi/Filter 0.5 pCi/Filter Run: ALPHANAL YST _120723A -Sample was not spiked and is reported as a Duplicate. All tracer recoveries are acceptable therefore the batch is approved. Sample 10: LCS-34240 Thorium 230 Laboratory Control Sample 0.1 pCi/Filter Run: ALPHANAL YST _120723A 80 120 -Sample was not spiked. All tracer recoveries are acceptable therefore the batch is approved. Sample 10: MB-34300 Thorium 230 Thorium 230 precision (±) Thorium 230 MDC Qualifiers: RL -Analyte reporting limit. 3 Method Blank 0.1 pCi/Filter 0.08 pCi/Filter 0.09 pCi/Filter MDC -Minimum detectable concentration Run: ALPHANAL YST _120723A N D -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. 69 07/25/12 11 :39 123.2 07/25/12 11 :39 S 07/25/12 11 :39 Page 16 of 22 EN:RGY LABORATORIES www.energylab.com Analytical ExCSOBflCII Sines 1952 Helena, MT 877-472-0711 • Billings, MT 800~735-4489 • Casper, WY 888-235-0515 Gillette, WY 866-686-7175 • Rapid City, SD 88B~672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 2nd Quarter Air 2012 Analyte Count Result Units Method: E909.0 Sample 10: MB-16745 Lead 210 Lead 210 precision (±) Lead 210 MDC Sample 10: LCS-16745 Lead 210 Sample 10: C12070341-006AMS Lead 210 Sample 10: C12070341-006AMSO Lead 210 Qualifiers: RL -Analyte reporting limit. 3 Method Blank 2 pCi/Filter 5 pCilFilter 8 pCi/Filter Laboratory Control Sample 741 pCi/Filter Sample Matrix Spike 2300 pCi/Filter Sample Matrix Spike Duplicate 2420 pCi/Filter MDC -Minimum detectable concentration Report Date: 08/10/12 Work Order: C12070341 RL %REC Low Limit High Limit Run: SUB-T46565 Run: SUB-T46565 96 70 130 Run: SUB-T46565 99 70 130 Run: SUB-T46565 105 70 130 NO -Not detected at the reporting limit. RPO RPOLimit Qual 5.2 Batch: T_16745 07/31/1207:48 U 07/31/1208:35 07/31/1214:31 07/31/1215:19 15.2 U -Not detected at minimum detectable concentration Page 17 of 22 EN:RGY www.energylab.com Helena, MT 871-412-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 .~iUett.e,WY 8&6 .. &86-7115 • Rapid City, S[) 888-672-1225 • College Station, IX 888-690-2218 LABORATORIES Analytical ExCBnsncB Sines 1:952 Client: Denison Mines USA Corp Project: 2nd Quarter Air 2012 QA/QC Summary Report Prepared by Casper, WY Branch Report Date: 08/10/12 Work Order: C12070341 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW6020 Sample 10: ICV Uranium Sample 10: ICSA Uranium Sample 10: ICSAB Uranium Method: SW6020 Sample 10: MB-34300 Uranium Sample 10: LCS2-34300 Uranium Sample 10: C12070341-001AMS Uranium Sample 10: C12070341-001 AMSO Uranium Sample 10: C12070341-006AOIL Uranium Qualifiers: RL -Analyte reporting limit. MDC -Minimum detectable concentration Initial Calibration Verification Standard 0.0508 mg/L 0.00030 Interference Check Sample A 5.17E-05 mg/L 0.00030 Interference Check Sample AB 1.20E-05 mg/L 0.00030 Method Blank 6E-05 mglfilter Laboratory Control Sample 0.0978 mglfilter 0.0028 Sample Matrix Spike 0.868 mglfilter 0.0028 Sample Matrix Spike Duplicate 0.862 mglfilter 0.0028 Serial Dilution 0.00562 mglfilter 0.014 Analytical Run: ICPMS4-C_120803A 08/03/12 21 :14 102 90 110 Run: ICPMS4-C_120803A Run: ICPMS4-C_120803A 98 85 115 Run: ICPMS4-C_120803A 100 75 125 Run: ICPMS4-C_120803A 99 75 125 Run: ICPMS4-C_120803A 0.7 08/03/1221 :18 08/03/1221 :23 Batch: 34300 08/04/12 17:49 08/04/12 17:53 08/04/12 18:07 08/04/12 18:30 20 08/04/12 19:01 20 NO -Not detected at the reporting limit. Page 18 of 22 ,"" www.energylab.com ' m:J'" ' ~~ AlIaIyticaI!xCSIISflCIlSiI1CB 1952 .1 Helena, MT 817 .. 472-11711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 GfII~tie,WV 866-686-7175 • Rapid City, so 888-&72-1225 • College Station, TX 888-690-2218 Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Den ison Mines USA Corp Login completed by: Tracy Judge Reviewed by: SL2000\tparke Reviewed Date: 7/24/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Container/Temp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: Yes 0' Yes 0 Yes 0 Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' Yes 0' 'C NA Yes 0 Yes 0 C12 070341 Date Received: 7/11/2012 Received by: tj No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Carrier NDA name: Not Present 0 Not Present 0' Not Present 0' No VOA vials submitted 0' Not Applicable 0' Cli ent contacted to confi rm that SHV -3 should not have been listed on the COC. T J 7/11/12. Page 19 of 22 "U Q.) co CD I\) o o -I\) I\) EI\ERGY mJ-',- Page -L-of ---i--"" Chain of Custody and Analytical Request Record Company Name: D e..A." .s C> .A. .;V\ ~ v'\ e-..s Report Mail Address: Po R 0 )< ~ 0 q IS \~A.~~ "'\5 1 VI q ... , 51 J I nvoice Address: S &-..LI'-"'-!.- Special ReportlF ormats: Dow o EOO/EDT(Electronic Data) o POTWNVWTP Format: ___ _ o State: D LEVEL IV o Other: ----o NELAC 2 3 ---- SAMPLE IDENTIFICATION JName, LQcation, Interval, e!Ql 13HV-1 Ktt~ B'Hv-3 4 EI-t\! -L1 5 J3Hv-5 6 131--1 \/-6 Collection Collection Date Time L-f/3/1 2h7/~h~ A\ ! t I _w ! J, 7 ()' o...lA. t. 1-1/5/) ~q/~/I~ 8 9 10 Custody Record Relinquished by (pnnt): 6~rt"\ II\. fA.J.-u- Relinquished bylprint): DatelTime: 7/;..~t '-\\ 00 DatefTime: PLEASE PRINT (Provide as much information as possi~I~J Project Name, PWS, Permit, Etc. I Sample Origin 2 ~~ o v 0... , te,r A ~r ~o \ ~ State: Ul Contact Name: Phone/Fax' . . Email: 6tLrf"~~ Pe.,..IVV\e.f' 1-i35 67i ;;2~;Z \ Invoice Contact & Phone: Purchase Order: DiXv ~ J. T ur-l'-Li3b t7( -;2 ~;2.1 EPNState Compliance: Yes ~ No 0 Sampler: (Please Print) 6-t-r f'~"'" P "" I ~e.r Quote/Bottle Order: 3: ~[b W@U@ OO§®C!JJ§@1ff§1]) '-1 Contact ELI prior to RUSH sample submittal o '-~o(/)~ cCO-C~1 "-._>;.:V Q) ~(f)~ m~ 83:=arJ 0) ..... « (f)1·Q .~ o '-co.l~ ~'-Qj,S c::.§ 0.(1)00 >.:>1;;; F-> (\) • ::::l Q).~ 11) ~ Z-o.«lo>o E ~I ~ MATRIX r3-A l' \ ) ( \i i3-A ~:~; )(IXI'><I)( ~ I )(' I ){ I ". >Clil)(l)( )(IXlxlx )(1)(1)c1~ ~I){I~I>< )( 1)( 1)( 1;< Signature: 6-~P~ Signature: bD~ [ R for charges and 0 scheduling -See W Instruction Page ::c "0 () c: Comments: ::::l U « 0 ~"..1-e.J. '-t-tU (.0 l'G.(.}i OA ~ c: '-L.l/ >/ l ~ +\""H1VJ>" ::::l ~ 5 w "E '7/:2./ f ~ W cu . (f) "0 c: ct1 -' H (f) ReceiPtTemp;;e." , 2t-,z.. 0 c On Ice: Y 6 Custody Seal~ On Bottle y t( On Cooler N Intact N Signature ~ N Match ~ II~ \fcf,~l r~\~td. \D '}11 JIC) ~ Received by (print): DatefTime: Received by (print): OatelTime: ~ I~ ~ ~ CO) ~ ~ ~ ta) ~~J~aM't\ I~ Signature: Signature: MUSTber--------------------------------4~~~~----~~------~~~------~ Signed Sample Disposal:_ Return to Client: Lab Disposal: ___ ._. __ In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order ~r:J.. e tqalYSiS requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical r~'" Visit our web site at www.enen:wlap.com for additional information. downloadable fee schedule. forms. and links. ATTACHMENT D AIR PARTICULATE LOADING GRAPHS AND SUPPORTING DATA 0 0 0 ~ !-" 0 0 0 ...... 0 0 0 ...... 0 0 0 ...... 0 0 0 ...... 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 10/5/2009 11/5/2009 l> t 12/5/2009 -. ..., OJ 1/5/2010 V) :c P+ < 2/5/2010 OJ I P+ ...... -. 3/5/2010 + 0 4/5/2010 :::s OJ 5/5/2010 ""C :c OJ < 6/5/2010 ..., N P+ -. + 7/5/2010 n 8/5/2010 C OJ OJ 9/5/2010 P+ :c to < ~ 10/5/2010 r- + 11/5/2010 0 OJ 12/5/2010 c.. OJ :::s :c 1/5/2011 < C1Q Ln 2/5/2011 ........ f 3/5/2011 3 4/5/2011 C1Q OJ ............. :c 5/5/2011 3 < en 6/5/2011 w .......... 7/5/2011 8/5/2011 9/5/2011 10/5/2011 11/5/2011 12/5/2011 1/5/2012 2/5/2012 3/5/2012 4/5/2012 5/5/2012 6/5/2012 0 0 ~ ..... 0 0 ..... 0 0 ..... 0 0 ..... 0 0 0 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 10/5/2009 11/5/2009 12/5/2009 Ol 1/5/2010 ::I: 2/5/2010 < I 3/5/2010 ...,a. 4/5/2010 -a OJ 5/5/2010 ""'" ~ -- 6/5/2010 n t: t 7/5/2010 OJ - 8/5/2010 ~ n> OJ 9/5/2010 I r-< 0 I 10/5/2010 ..... OJ 11/5/2010 C. 12/5/2010 ::::J C1Q 1/5/2011 ......... 2/5/2011 3 3/5/2011 C1Q .............. 4/5/2011 3 5/5/2011 -w ........ 6/5/2011 7/5/2011 8/5/2011 9/5/2011 10/5/2011 11/5/2011 12/5/2011 1/5/2012 2/5/2012 3/5/2012 4/5/2012 5/5/2012 6/5/2012 0 0 !=> ...... 0 0 ...... 0 0 ...... 0 0 ...... 0 0 0 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 10/5/2009 11/5/2009 12/5/2009 D' 1/5/2010 :::I: 2/5/2010 < I 3/5/2010 N 4/5/2010 -0 QJ 5/5/2010 .., r+ -- 6/5/2010 n C + 7/5/2010 QJ 8/5/2010 r+ tD OJ 9/5/2010 I r-< 0 N 10/5/2010 QJ 11/5/2010 a.. 12/5/2010 ::::s C7Q 1/5/2011 -.......... 2/5/2011 3 C7Q 3/5/2011 ............... 4/5/2011 3 5/5/2011 w ~ 6/5/2011 7/5/2011 8/5/2011 9/5/2011 10/5/2011 11/5/2011 12/5/2011 1/5/2012 2/5/2012 3/5/2012 4/5/2012 5/5/2012 6/5/2012 0 0 0 ~ ~ 0 0 0 ~ 0 0 0 ~ 0 0 0 ~ 0 0 0 ~ 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 10/5/2009 11/5/2009 12/5/2009 D' 1/5/2010 % 2/5/2010 < I 3/5/2010 ~ 4/5/2010 "'tJ OJ 5/5/2010 .., ,.... -. 6/5/2010 n c: + 7/5/2010 OJ 8/5/2010 ,.... (1) OJ 9/5/2010 :c r-< 0 ~ 10/5/2010 OJ 11/5/2010 c.. 12/5/2010 ::::J CJQ 1/5/2011 ......... 2/5/2011 3 3/5/2011 CJQ .............. 4/5/2011 3 5/5/2011 w ~ ;;;:==+' .......-. 6/5/2011 ~I 7/5/2011 8/5/2011 9/5/2011 10/5/2011 11/5/2011 12/5/2011 1/5/2012 2/5/2012 3/5/2012 4/5/2012 5/5/2012 6/5/2012 0 0 !=> ...... 0 0 ...... 0 0 ...... 0 0 ...... 0 0 0 0 0 0 0 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 10/5/2009 11/5/2009 12/5/2009 g, 1/5/2010 ::I: 2/5/2010 < I 3/5/2010 U'I 4/5/2010 -a Q,J 5/5/2010 .., r+ -- 6/5/2010 n c: + 7/5/2010 Q,J 8/5/2010 r+ (1) OJ 9/5/2010 :c r-< 0 Ln 10/5/2010 Q,J 11/5/2010 c.. 12/5/2010 ::::s C7Q 1/5/2011 . ......-. 2/5/2011 3 3/5/2011 C7Q ............... 4/5/2011 3 5/5/2011 w -...,.... 6/5/2011 7/5/2011 8/5/2011 9/5/2011 10/5/2011 11/5/2011 12/5/2011 1/5/2012 2/5/2012 3/5/2012 4/5/2012 5/5/2012 6/5/2012 1/5/2009 2/5/2009 3/5/2009 4/5/2009 5/5/2009 6/5/2009 7/5/2009 8/5/2009 9/5/2009 10/5/2009 11/5/2009 12/5/2009 1/5/2010 2/5/2010 3/5/2010 4/5/2010 5/5/2010 6/5/2010 t 7/5/2010 8/5/2010 OJ 9/5/2010 :c < en 10/5/2010 11/5/2010 12/5/2010 1/5/2011 2/5/2011 3/5/2011 4/5/2011 5/5/2011 6/5/2011 7/5/2011 8/5/2011 9/5/2011 10/5/2011 11/5/2011 12/5/2011 1/5/2012 2/5/2012 3/5/2012 4/5/2012 5/5/2012 6/5/2012 0 a 0 I-> 0 o a I-> o o ~ I-> o o o I I-> a o o o D' ::I: < I en '1:J OJ .., ,.... -. n c: OJ ,.... tD r-o OJ c.. :::s C7Q ......... 3 C7Q ~ 3 w ~ ~ek If 1 2 3 4 5 5 7 g ~ 0 1 2 3 1 2 3 4 5 3 7 3' 3 0 1 2 3 If 1 2 3 4 5 3 7 3 3 0 1 2 3 1 2 3 4 5 3 7 3 3 0 1 2 3 BHV-1 on stream % Filter Start Number Date 8399966 3-Jan-12 8399957 09-Jan-12 8399951 16-Jan-12 8399945 23-Jan-12 8399940 30-Jan-12 8399933 06-Feb-12 8399927 13-Feb-12 8399921 20-Feb-12 8399915 27-Feb-12 8399909 05-Mar-12 8399903 12-Mar-12 8401196 19-Mar-12 8401190 26-Mar-12 Totals 91 BHV-2 on stream % Filter b Num er 8399965 8399958 8399952 8399946 8399941 8399934 8399928 8399922 8399916 8399910 8399904 8401197 8401191 Totals Start Date 03-Jan-12 09-Jan-12 16-Jan-12 23-Jan-12 30-Jan-12 06-Feb-12 13-Feb-12 20-Feb-12 27-Feb-12 05-Mar-12 12-Mar-12 19-Mar-12 26-Mar-12 91 BHV-4 on stream % Filter Start Number Date 8399964 03-Jan-12 8399959 09-Jan-12 8399953 16-Jan-12 8399947 23-Jan-12 8399942 30-Jan-12 8399935 06-Feb-12 8399929 13-Feb-12 8399923 20-Feb-12 8399917 27-Feb-12 8399911 05-Mar-12 8399905 12-Mar-12 8401198 19-Mar-12 8401192 26-Mar-12 Totals 91 BHV-5 on stream % Filter b Num er 8399963 8399960 8399954 8399948 8399943 8399936 8399930 8399924 8399918 8399912 8399906 8401199 8401193 Totals Start D ate 03-Jan-12 09-Jan-12 16-Jan-12 23-Jan-12 30-Jan-12 06-Feb-12 13-Feb-12 20-Feb-12 27-Feb-12 05-Mar-12 12-Mar-12 19-Mar-12 26-Mar-12 91 100.1% Stop Date 9-Jan-12 16-Jan-12 23-Jan-12 30-Jan-12 6-Feb-12 13-Feb-12 20-Feb-12 27-Feb-12 5-Mar-12 12-Mar-12 19-Mar-12 26-Mar-12 3-Apr-12 2184.0 100.1% Stop Date 09-Jan-12 16-Jan-12 23-Jan-12 30-Jan-12 06-Feb-12 13-Feb-12 20-Feb-12 27-Feb-12 05-Mar-12 12-Mar-12 19-Mar-12 26-Mar-12 03-Apr-12 2184.0 99.9% Stop Date 09-Jan-12 16-Jan-12 23-Jan-12 30-Jan-12 06-Feb-12 13-Feb-12 20-Feb-12 27-Feb-12 05-Mar-12 12-Mar-12 19-Mar-12 26-Mar-12 03-Apr-12 2184.0 99.9% Stop D ate 09-Jan-12 16-Jan-12 23-Jan-12 30-Jan-12 06-Feb-12 13-Feb-12 20-Feb-12 27-Feb-12 05-Mar-12 12-Mar-12 19-Mar-12 26-Mar-12 03-Apr-12 2184.0 Gross 4.2823 4.3496 4.3816 4.3144 4.3245 4.3239 4.2776 4.3323 4.3652 4.8686 4.6229 4.5338 4.6642 4.4339154 G ross 4.5105 4.5563 4.3810 4.3396 4.3922 4.3713 4.3032 4.3064 4.3739 4.8945 4.8445 4.6060 4.7934 4.513292 Gross 4.2723 4.2589 4.3706 4.3025 4.2199 4.2594 4.2509 4.3665 4.3172 4.6349 4.4881 4.4475 4.5856 4.367254 G ross 4.3257 4.4223 4.4607 4.3395 4.3451 4.3095 4.2985 4.3473 4.3753 4.8772 4.6137 4.5574 4.7400 4.462477 Tare Net 4.2156 0.0667 4.2768 0.0728 4.2657 0.1159 4.2592 0.0552 4.2340 0.0905 4.2361 0.0878 4.2147 0.0629 4.2064 0.1259 4.2330 0.1322 4.2356 0.6330 4.2600 0.3629 4.3852 0.1486 4.3574 0.3068 4.259977 0.1739 T are N et 4.2287 0.2818 4.2493 0.3070 4.2266 0.1544 4.2434 0.0962 4.2369 0.1553 4.2245 0.1468 4.2115 0.0917 4.1337 0.1727 4.2285 0.1454 4.2577 0.6368 4.2798 0.5647 4.3797 0.2263 4.3043 0.4891 4.24651 0.2668 Tare Net 4.2466 0.0257 4.2017 0.0572 4.2472 0.1234 4.2767 0.0258 4.1668 0.0531 4.1820 0.0774 4.2076 0.0433 4.2227 0.1438 4.2462 0.0710 4.2460 0.3889 4.2385 0.2496 4.3597 0.0878 4.3638 0.2218 4.24658 0.1207 T are N et 4.2449 0.0808 4.2435 0.1788 4.2832 0.1775 4.2716 0.0679 4.2408 0.1043 4.2020 0.1075 4.2128 0.0857 4.2167 0.1306 4.2120 0.1633 4.1741 0.7031 4.2469 0.3668 4.3895 0.1679 4.3779 0.3621 4.25507 0.2074 Stop Time 35231.9 35398.5 35567.6 35736.4 35905.5 36072.9 36239.8 36409.9 36580.4 36743.3 36914.5 37081.1 37274.8 Stop T Ime 45418.1 45585.8 45753.4 45922.8 46091.4 46259.3 46425.8 46596.3 46766.9 46929.3 47100.9 47267.5 47461.3 Stop Time 20749.4 20916.2 21083.9 21254.0 21421.7 21589.7 21757.2 21926.7 22097.1 22260.6 22432.0 22597.8 22789.9 Stop T Ime 44756.8 44923.5 45091 .2 45261.3 45429.6 45597.4 45764.9 45933.6 46104.2 46268.3 46439.7 46605.5 46797.1 BHV-1 Start Time 35089.2 35231.9 35398.5 35567.6 35736.4 35905.5 36072.9 36239.8 36409.9 36580.4 36743.3 36914.5 37081.1 BHV-2 Start T Ime 45275.8 45418.1 45585.8 45753.4 45922.8 46091.4 46259.3 46425.8 46596.3 46766.9 46929.3 47100.9 47267.5 BHV-4 Start Time 20607.8 20749.4 20916.2 21083.9 21254.0 21421.7 21589.7 21757.2 21926.7 22097.1 22260.6 22432.0 22597.8 BHV-5 Start T Ime 44615.0 44756.8 44923.5 45091.2 45261.3 45429.6 45597.4 45764.9 45933.6 46104.2 46268.3 46439.7 46605.5 Total Time 8560.8 9995.4 10147.2 10123.2 10149.0 10045.2 10009.8 10207.8 10231.8 9771.6 10273.2 9998.4 11619.0 131132.4 Total T Ime 8535.0 10064.4 10057.2 10164.0 10116.6 10072.8 9989.4 10229.4 10233.6 9748.2 10292.4 9998.4 11629.8 131131.2 Total Time 8498.4 10008.6 10062.6 10201.2 10064.4 10078.8 10048.8 10170.0 10225.8 9812.4 10279.2 9951.6 11527.2 130929 Total T Ime 8511.0 10001.4 10063.8 10203.6 10096.2 10068.0 10050.0 10122.0 10240.2 9847.2 10279.8 9949.8 11496.6 130929.6 Total Volume: 4.82E+06 Total Loading, Per Cent Liters mg/m3 On Stream 8,848,143 0.0075 99.1% 10,472,414 0.0070 99.2% 10,631,458 0.0109 100.7% 10,606,313 0.0052 100.4% 10,633,344 0.0085 100.7% 10,524,590 0.0083 99.7% 10,459,156 0.0060 99.3% 10,666,045 0.0118 1Ol.3% 10,691,122 0.0124 101.5% 10,127,253 0.0625 96.9% 10,588,929 0.0343 101.9% 10,305,683 0.0144 99.2% 11,976,089 0.0256 100.9% 136,530,540 0.0165 100.1% 99927 4.82E+06 Total L· Iters 8,821,477 10,544,707 10,537,163 10,649,060 10,599,398 10,553,508 10,437,841 10,688,615 10,693,003 10,103,001 10,608,719 10,305,683 11,987,221 136,529,395 mgJm n tream Loading, Per Cent / 3 0 S 0.0319 98.8% 0.0291 99.8% 0.0147 99.8% 0.0090 100.8% 0.0147 100.4% 0.0139 99.9% 0.0088 99.1% 0.0162 101.5% 0.0136 101 .5% 0.0630 96.7% 0.0532 102.1% 0.0220 99.2% 0.0408 101.0% 0.0255 100.0% Total Volume: 4.81 E+06 Total Loading, Per Cent Liters mg/m3 On Stream 8,783,648 0.0029 98.4% 10,486,244 0.0055 99.3% 10,542,821 0.0117 99.8% 10,688,035 0.0024 101.2% 10,544,707 0.0050 99.8% 10,559,794 0.0073 100.0% 10,499,907 0.0041 99.7% 10,626,548 0.0135 100.9% 10,684,853 0.0066 101.4% 10,169,538 0.0382 97.3% 10,595,113 0.0236 102.0% 10,257,445 0.0086 98.7% 11,881,468 0.0187 100.1% 136,320,121 0.0114 99.9% Total Volume: 4.81 E+06 Total U I ers 8,796,671 10,478,700 10,544,078 10,690,550 10,578,024 10,548,479 10,501,161 10,576,393 10,699,900 10,205,605 10,595,731 10,255,589 11,849,928 136,320,809 Loading, Per Cent / 3 0 St mglm n ream 0.0092 98.5% 0.0171 99.2% 0.0168 99.8% 0.0064 101.2% 0.0099 100.2% 0.0102 99.9% 0.0082 99.7% 0.0123 100.4% 0.0153 101.6% 0.0689 97.7% 0.0346 102.0% 0.0164 98.7% 0.0306 99.8% 0.0197 99.9% SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 Page 21 of 22 Period: Janurary 3,2012 through April 3, 2012(1stQuarter 2012) BHV-6 on stream % Filter Start Number Date 1 8399962 03-Jan-12 2 8399961 09-Jan-12 3 8399955 16-Jan-12 4 8399949 23-Jan-12 5 8399938 30-Jan-12 3 8399937 06-Feb-12 7 8399931 13-Feb-12 3 8399925 20-Feb-12 3 8399919 27-Feb-12 0 8399913 05-Mar-12 1 8399907 12-Mar-12 2 8401200 19-Mar-12 3 8401194 26-Mar-12 Totals 91 ALL BHV on stream % lek If. Blanks Start Date 1 8401195 03-Jan-12 2 8399950 09-Jan-12 3 8399944 16-Jan-12 4 8399939 23-Jan-12 5 8399932 30-Jan-12 3 8399926 06-Feb-12 7 8399920 13-Feb-12 3 8399914 20-Feb-12 3 8399908 27-Feb-12 0 8399902 05-Mar-12 1 8399901 12-Mar-12 2 8401 189 19-Mar-12 3 8401183 26-Mar-12 Totals 91 99.9% Stop Date 09-Jan-12 16-Jan-12 23-Jan-12 30-Jan-12 06-Feb-12 13-Feb-12 20-Feb-12 27-Feb-12 05-Mar-12 12-Mar-12 19-Mar-12 26-Mar-12 03-Apr-12 2184.0 100.0% Stop Date 09-Jan-12 16-Jan-12 23-Jan-12 30-Jan-12 06-Feb-12 13-Feb-12 20-Feb-12 27-Feb-12 05-Mar-12 12-Mar-12 19-Mar-12 26-Mar-12 03-Apr-12 2184.0 G ross 4.3221 4.3761 4.3810 4.2582 4.3000 4.3130 4.3075 4.3082 4.3253 4.7666 4.5700 4.5046 4.6227 4.411946 Net 4.3631 4.2523 4.2780 4.2005 4.1773 4.2076 4.2176 4.2437 4.2609 4.2101 4.2788 4.3604 4.3931 4.2649 T are N et 4.2208 0.1013 4.2625 0.1136 4.2564 0.1246 4.2013 0.0569 4.2074 0.0926 4.2165 0.0965 4.2346 0.0729 4.1935 0.1147 4.2103 0.1150 4.2421 0.5245 4.2725 0.2975 4.3877 0.1169 4.3341 0.2886 4.24921 0.1627 Stop T !me 10655.7 10822.2 10989.9 11160.0 11327.5 11495.6 11663.1 11832.6 12002.9 12166.6 12337.9 12503.8 12695.8 BHV-6 Start T !me 10513.7 10655.7 10822.2 10989.9 11160.0 11327.5 11495.6 11663.1 11832.6 12002.9 12166.6 12337.9 12503.8 Total T !me 8520.0 9989.4 10063.2 10202.4 10054.2 10084.2 10048.2 10171.2 10219.2 9820.2 10279.8 9951.0 11520.6 130923.6 Page 2 Total Volume: 4.81 E+06 Total L· !ters 8,805,973 10,466,128 10,543,450 10,689,293 10,534,020 10,565,452 10,499,280 10,627,802 10,677,957 10,177,622 10,595,731 10,256,826 11,874,665 136,314,198 mglm n tream Loading, Per Cent / 3 0 S 0.0115 98.6% 0.0109 99.1% 0.0118 99.8% 0.0053 101.2% 0.0088 99.7% 0.0091 100.0% 0.0069 99.7% 0.0108 100.9% 0.0108 101.4% 0.0515 97.4% 0.0281 102.0% 0.0114 98.7% 0.0243 100.0% 0.0155 99.9% SCFM 36.5 37.0 37.0 37.0 37.0 37.0 36.9 36.9 36.9 36.6 36.4 36.4 36.4 36.8 Page 22 of 22 ATTACHMENT E ENVIRONMENTAL GAMMA GRAPHS AND SUPPORTING DATA I White Mesa Mill Ambient Gamma Levels Over Time I 50.00 ,--------------------------------------------------------------------------------------------------------------------------, 45.00 -f------------------------------~------ 40.00 -f---------------------------------------------------------------------------------------------------------1-+---------.... ----------/ 35.00 -f----------------------------------------------------------------H---------------------------------------------------------------------------------:&-------------------------------/--+----------.a.----f--\--.. ------------------~ 30.00 L-ID t: 25.00 CO ::J 0" -E ID 0::: 20.00 E 15.00 1 0.00 -f-----/-I-------------------------.---------------------------------------------------------------------.--/-\-- 5.00 I _1-V-W\tI9"--....dII--f--l-~-+\-F\___------f_w.--~-__/--+-----.. -------------;;;;; __ ---H +-I---J-I-----J-.l::-H------__a----------I-.-a.I.-II-&l-\-f--l--l-1 0.00 K1r zrr:r ~~ 30-Sep_81 05-J/JI_83 04-Apr_85 03-l=eb_8? 11-0ct_88 16-J/JI_90 10-Apr_92 13-Jan_94 16-0ct_95 8-J/JI_9? 13-A.pr_99 20_l=eb_O 1 15-0ct_02 9-J/JI_04 10-Apr_06 31-Dec_O? 2-0ct-09 1;1;1-11/£ M£SA. MILL Background (BHV-3) subtracted from BHV-1, BHV-2, BHV-4, BHV-5, and BHV--6 --..-SHV-1 -+-SHV-2 """'-SHV-3 _SHV-4 _SHV-5 ~SHV-6 ! White Mesa Mill Ambient Gamma Levels Over Time BHV-1! 50.00 ~------------------------------------------------------------------------------------------------------------------------~ 45.00 1 --------------------------.------------------------------------------------1 40.00 +------------------------------------------.-------------------------------------.---------.------------------.----------.-----------------------------1 35.00 -1------ 30.00 s.... Q) t co 25.00 :::J 0'" -E Q) 0::: 20.00 E 15.00 10.00 ..f --------.-------------------------------------1-\ 0.00 I ~ it" i .. , "~" ~ III ,~' 1I1111111111i ,'~II i="" II'''' tie .. SIIA IIRi='t IIIIIF"7", ,', ,,16 ,', ","7",," , " , " , ," '",I 30~S 03~O 07~O 09~O 30~O 30~S 8-0ct ep-81 ct~83 ct~85 ct~87 ct~89 ep~91 ~93 16~Oct~95 10~Nov~97 12~Oct~99 24~Oct~01 3~Oct~03 17~Oct~05 30~Oct~07 2~Oct~09 DIR12CI R.4DIA liON Background (BHV-3) Subtracted from BHV-1 --'-'BHV-1 '"-Q) t CO ::J 0--E Q) 0:: E I White Mesa Mill Ambient Gamma Levels Over Tim; BHV-21 50.00 ~----------------------------------------------------------------------------------------------------------~ 45.00 +I----------------------------------------------------------------------------------------------------~ 40.00 +I----------------------------------------------------------------------------------------------------~ 35.00+1---------------------------------------------------------------------------------------------------4 30.00 25.00 20.00 15.00 10.00 I • 5.00 I n 1\ 'I . • .. 1'f 0.00 .. ftll7~.,it;:ttj ,.~.,., Ili¥,laF Ii iii " ,-,.,..II~ .. ~.~~~II~ ~.'~~'" '..-,., ill! 30~S 03~O O?~o 09~O 30~O 30~S 8~Oct ep~81 ct~83 ct~85 ct~8? ct~89 ep~91 ~93 16~Oct~95 10~Nov~9? 12~Oct~99 24~Oct~01 3~Oct~o3 1?~Oct~05 30~Oct~O? 2~Oct~09 DIR£cI f?A.D IAIION Background (BHV-3) Subtracted from BHV-2 ___ BHV-2 -------] I White Mesa Mill Ambient Gamma Levels Over Time BHV-31 50.00 45.00 40.00 35.00 30.00 "-(],) t ro ::J 0--E (],) 0::: E 20.00 15.00 -\--------------------------l-/------------------------------------------------------------------------------------------------------------------------------------_____________________________________________ lI!II1. ________ -------------------------------------------------------------------------------------------------------------------------1 10.00 i---------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------/ 5.00 i--------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------1 0.00 " ',' ',-, ,-,' ,-,- 30-Sep_81 03-0Ct_83 0?-OCt_85 09_0ct_8? 30-0Ct_89 30-S 8-0ct ep-91 -93 Background (BHV-3) 16_0ct_ 95 10-Nov_9? 12-0ct_99 24-0Cf_01 3-0ct_03 1?_Oct_05 30-0ct_O? 2-0 ct_09 DIRECT R4D/4 TtON --'-BHV-3 s.... ~ ro :::l 0'" E Q) ~ E I White Mesa Mill Ambient Gamma Levels Over Time BHV-41 50.00 ~------------------------------------------------------------------------------------------------------------------------------~ 45.00 ~I----------------------------------------- 40.00 +-------------------------.-------------------------.. -----------.. -.------------.. ---------.-------.-------.-----.--... ---.. -.. ----.-----------.-----.-------------------------~ 35.00 +1--- 30.00 001---------~ 25.00 +----.-.-----------------------. -I 20.00 ~ -.--------------------------------------------------------------------------1 15.00 -I -.----.---------------------------.. ------.-----------------·---·-··---·------·--··--------·--------------1 10.00 +---I , -------.------- 5.00 " ~, " ii· ... ,'.-.-llli ~"'Ii ', ",,~ il ~'_ ' ... ~. ~, .. ' Iii '1i 'W:;:;:; w: ~" ;:s-Ilf ~ "Ii .' 0.00 ~ ~. , --- 30-Sep_81 03-0Ct_83 07_0Ct_ 85 09_0Ct_ 87 30-0Ct_89 30-Sep_91 8-0ct-93 16-0ct_95 10-Noll_97 12-0Cf_99 24-0ct_01 3-0ct-03 17_0ct_ 05 30-0Ct_07 2-0Cf-09 DIR.£cr RADIAItON Background (BHV-3) Subtracted from BHV-4 --+-BHV-4 I White Mesa Mill Ambient Gamma Levels Over Time BHV-sl 50.00 ~------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------~ 45.00 +1-----------------------------------------------------------------------------------------------------------~ 40.00 +1--------------------------------------------------------------------------------------------------------------~ 35.00 +I------------~--------------------------------------------------------------------------------------------~ 30.00 ~ Q) t CO ::::J 25.00 0--E Q) 0:: E 20.00 15.00 +1----------------------------------------------------------------------------------------------------------~ 10.00 1 1------------------------------------------------------------------1·~--~----_=--------------------------~~ 5.00 1 I I ,. ___ I ~'" R 1"'\ , .... 'T\oA I I _ I I 1 I I :l." .. II I II 0.00 ".ii ~i ::'.i i ••• i i .i .i i .i iii ii i i .i ii.i iii iiiii i _i ~'i ;"!;\ i'i i " 30~Sep~81 03~Oct~83 07~Oct~85 09~Oct~87 30~Oct~89 30~Sep~91 8~OCt~93 16~Oct~95 10~tvOI/~97 12~Oct~99 24~Oct~01 3~Oct~03 17~Oct~05 30~Oct~07 2~Oct~09 D1REc, RA. DIA./fOtv Background (BHV-3) Subtracted from BHV-5 -'-BHV-5 ! White Mesa Mill Ambient Gamma Levels Over Time BHV-S! 50.00 45.00 40.00 ----------------~-"--------------------------- 35.00 ------------ 30.00 ------------- L-a.> t ro 25.00 :::J 0--E a.> 0::: 20.00 ----------------------------------------"-------"----"---------------------------------------------,---------_ •.•. _--------------_._-_ ... _--------------_ ... _-----._-------------------------_._--------"-----_.- E 15.00 -----------------------_._-------------,- 10.00 -------------------------------- 5.00 0.00 30-Sep_81 03-0CI_83 O?-OCI_85 09-0CI_8? 30_0CI_89 30-Sep_91 8-0CI_93 16-0CI_95 10-Nov_9? 12-0CI_99 24-0CI_01 3-0CI_03 1?-OCI_05 30-0CI_O? 2-0CI_09 DIR£cr RADIA /JON Background (BHV-3) Subtracted from BHV-6 -'-BHV-6 Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 51 52 53 64 White Mesa Mill Second Quarter 2012 Environmental Spherical Gamma Monitor Results Mean Location Administration Vault V205 Control Room BHV-6 Ore Stor. -Molycorp Area Vanadium Precip.Area Yellocake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room Trommel Screen (ore pad) North East Comer Ore Pad Met. Lab Filter Press Room BHV-l BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scalehouse Sample Plant (OBS) Front Gate AF -Barrel Dump Station AF Circuit -South AF Circuit -North North Control # 1 North Control # 2 CaF2 Barrel Dump Station - Operator Station KF Barrel Dump Station Date Issued 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/312012 4/312012 4/312012 4/312012 4/312012 4/3/2012 4/3/2012 4/312012 4/312012 4/3/2012 4/3/2012 4/3/2012 4/312012 4/3/2012 4/312012 4/3/2012 4/312012 4/312012 4/312012 4/312012 4/312012 4/312012 4/312012 4/312012 4/312012 4/312012 4/312012 4/312012 4/312012 4/3/2012 4/312012 4/3/2012 4/3/2012 4/3/2012 4/312012 4/312012 4/3/2012 4/3/2012 Total Days Badge at Date Returned WMM 6/26/2012 84 6126/2012 84 612612012 84 6/26/2012 84 6/26/2012 84 612612012 84 612612012 84 6/26/2012 84 6/2612012 84 6/2612012 84 612612012 84 6/26/2012 84 612612012 84 6/2612012 84 612612012 84 612612012 84 6/2612012 84 612612012 84 6126/2012 84 612612012 84 612612012 84 612612012 84 6126/2012 84 6126/2012 84 6/26/2012 84 6/26/2012 84 612612012 84 6126/2012 84 6126/2012 84 612612012 84 6/26/2012 84 6/2612012 84 6/2612012 84 6/2612012 84 6/26/2012 84 6/2612012 84 6/26/2012 84 6/2612012 84 612612012 84 612612012 84 6/2612012 84 612612012 84 Ambient Dose Equivalent 38.2 o 32.6 340.5 92.5 144.1 197.6 327.9 186.2 76.5 165.3 237.3 71.1 170.9 38.6 31.6 31.1 35.1 37.5 404.4 59 76.6 61.7 42.1 92.9 1219.8 439.6 127.9 66.3 118.7 50.4 366.8 259 320.2 225 152.6 66.6 131.9 44.7 35.3 243.2 149.3 mReml hour 0.02 0.00 0.02 0.17 0.05 0.07 0.10 0.16 0.09 0.04 0.08 0.12 0.04 0.08 0.02 0.02 0.02 0.02 0.02 0.20 0.03 0.04 0.03 0.02 0.05 0.61 0.22 0.06 0.03 0.06 0.03 0.18 0.13 0.16 0.11 0.08 0.03 0.07 0.02 0.02 0.12 0.07 mRem/Day 0.455 0.000 0.388 4.054 1.101 1.715 2.352 3.904 2.217 0.911 1.968 2.825 0.846 2.035 0.460 0.376 0.370 0.418 0.446 4.814 0.702 0.912 0.735 0.501 1.106 14.521 5.233 1.523 0.789 1.413 0.600 4.367 3.083 3.812 2.679 1.817 0.793 1.570 0.532 0.420 2.895 1.777 mReml Week 3.18 0.00 2.72 28.38 7.71 12.01 16.47 27.33 15.52 6.38 13.78 19.78 5.93 14.24 3.22 2.63 2.59 2.93 3.13 33.70 4.92 6.38 5.14 3.51 7.74 101.65 36.63 10.66 5.53 9.89 4.20 30.57 21.58 26.68 18.75 12.72 5.55 10.99 3.73 2.94 20.27 12.44 Badge Number Control 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 45 46 47 51 52 53 54 White Mesa Mill First Quarter 2012 Environmental Spherical Gamma Monitor Results Mean Location Administration Vault V205 Control Room BHV-6 Ore Stor. -Molycorp Area Vanadium Precip.Area Yellocake Drying Area Leach SAG Mill Control Room Yellowcake Precip. Central Control Room Trommel Screen (ore pad) North East Comer Ore Pad Met. Lab Filter Press Room BHV-l BHV-2 BHV-3 BHV-4 BHV-5 SAG Mill Tails CCD North SX Administration Building Admin Parking Lot Yellowcake Packaging Yellowcake Storage Bucking Room Mill Lunch Room South SX Mtce. Super.'s Office Ore Feed Grizzly Scalehouse Sample Plant (OBS) Front Gate AF -Barrel Dump Station AF Circuit -South AF Circuit -North North Control # 1 North Control # 2 Vault CaF2 Barrel Dump Station Total Days Ambient Badge at Dose Date Issued Date Returned WMM Equivalent 12/30/2011 413/2012 95 32.9 12/30/2011 413/2012 95 50.8 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 12/30/2011 413/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 4/3/2012 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 95 30.3 916.4 83.7 108.5 o 415.3 124.5 89.6 145.6 185 68.2 179.4 33.2 28.9 29.2 30.6 33.4 480 53.8 72.8 73.7 38.5 80.6 1325.7 469.5 106.6 65 125.1 53.3 353.7 234.7 302.7 167.1 215.5 102.9 98.9 34.1 28.2 o 266 mReml mReml hour mRem I Day Week 0.01 0.346 2.42 0.02 0.535 3.74 0.01 0.40 0.04 0.05 0.00 0.18 0.05 0.04 0.06 0.08 0.03 0.08 0.01 0.01 0.01 0.01 0.01 0.21 0.02 0.03 0.03 0.02 0.04 0.58 0.21 0.05 0.03 0.05 0.02 0.16 0.10 0.13 0.07 0.09 0.05 0.04 0.01 0.01 0.00 0.12 0.319 9.646 0.881 1.142 0.000 4.372 1.311 0.943 1.533 1.947 0.718 1.888 0.349 0.304 0.307 0.322 0.352 5.053 0.566 0.766 0.776 0.405 0.848 13.955 4.942 1.122 0.684 1.317 0.561 3.723 2.471 3.186 1.759 2.268 1.083 1.041 0.359 0.297 0.000 2.800 2.23 67.52 6.17 7.99 0.00 30.60 9.17 6.60 10.73 13.63 5.03 13.22 2.45 2.13 2.15 2.25 2.46 35.37 3.96 5.36 5.43 2.84 5.94 97.68 34.59 7.85 4.79 9.22 3.93 26.06 17.29 22.30 12.31 15.88 7.58 7.29 2.51 2.08 0.00 19.60 Lost Badge Lost Badge ATTACHMENT F VEGETATION GRAPHS, DATA TABLE, LABORATORY RESULTS AND QA/QC (Log Scale) ~ a a a a a a a 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 ex> ....... 0') CJ'1 ~ c..v I\,) 8/27/1981 8/27/1982 8/27/1983 8/27/1984 8/27/1985 8/27/1986 8/27/1987 8/27/19881 -~ ......... :::0 Q) 8/27/19891 I ~ I N N 8/27/19901 ~ 0) (') 8/27/19911 ~ 0 ::l 0 8/27/1992 1 -i \. ~ (I) ::l .... .., 8/27/19931 ~I Q) .... 8/27/1994 o· f ::l tJ) 8/27/1995 ::l z m < 8/27/1996 (I) (Q t 8/27/1997 (I) .... Q) .... z 8/27/1998 o· ~ ::l 8/27/1999 -s:: f (') 8/27/2000 :::.: " (j) (Q ~ 8/27/2001 - 8/27/2002 8/27/2003 8/27/2004 8/27/2005 8/27/2006 8/27/2007 8/27/2008 8/27/2009 8/27/2010 8/27/2011 I I .: (Log Scale) a a a a a a a 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 ex> -.....J 0> CJ'1 ~ W N 8/27/1981 8/27/1982 8/27/1983 8/27/1984 8/27/1985 8/27/1986 8/27/1987 8/27/19881 I~ 1 "'tJ C'" 8/27/1989 i ... ~~ I N ~ 8/27/1990 i ~~ 1 0 0 8/27/1991 i I"" 0 :::J (') 8/27/1992 i ""'-1-.....-~ (I) :::J r+ -r= ., 8/27/1993 i ..... 1 D) e. 8/27/1994 0 t :::J en z 8/27/1995 :::J m < 8/27/1996 (I) (Q T 8/27/1997 (I) r+ D) r+ Z O· ~ 8/27/1998 :::J 8/27/1999 -c -,-f 0 8/-21-1-2880-~-i (j) (Q ~ 8/27/2001 - 8/27/2002 8/27/2003 8/27/2004 8/27/2005 8/27/2006 8/27/2007 8/27/2008 8/27/2009 8/27/2010 8/27/2011 (Log Scale) ~ a a a a a a a a a a a a a a m m m m m m m I I I I I I I a a a a a a a 00 -....I 0> (J'1 ~ w '" 01-Jan-81 01-Jan-82 ~ Ir-'-'.rr I ~ X o1-Jan-83 1 I =i m 01-Jan-84 s: m o1-Jan-85 1 ~I CA l> 01-Jan-86 s: o1-Jan-87 1 I ~ I r-r- 01-Jan-88 Z 01-Jan-89 i ~~ 0 ;;C -I 01-Jan-90 i ~ X m 01-Jan-91 i l..r _ ~ 1;; -I 01-Jan-92 0 t ." 01-Jan-93 s: AI 01 -Jan-94 r- oo -r-N 01 -Jan-95 ~;;C N 0) •• D) -. T 01-Jan-96 '::1\) CCI\) -0') "'U 01-Jan-97 D) 0-:::J N 01-Jan-98 c.. ->. 0 "'0 01-Jan-99 C'" • I\) 01-Jan-OO i ..---~ -0 01-Jan-01 i lJ! 1 ---0 0 :::J 01-Jan-02 i ~~ 0 (I) :::J 01-Jan-03 i •• .r-... .., D) 01 -Jan-04 i --....~ ... o· :::J 01 -Jan-051 UJ :::J 01-Jan-06 < (I) 01-Jan-07 i ~ --II CC (I) ... 01-Jan-08 i -I ~ D) ... 01-Jan-09 i I~ o· :::J 01 -Jan-10 01-Jan-11 01-Jan-12 (Log Scale) a a a a a a a 0 0 0 0 0 0 0 m m m m m m m I I I I I I I 0 0 0 0 0 0 0 OJ -....J 0) 01 ~ VJ I\.) 01-Jan-81 :E 01-Jan-82 -1 J..,./""' .rl ::I: =i 01-Jan-83 -1 .........--~ m s: 01 -Jan-84 -1 ......... -r--:JI m en 01-Jan-85 » s: 01-Jan-86 • • 01-Jan-87 Z 01...;Jan-88 0 :::c 01-Jan-89 -1 r----..... ____+__ -t ::I: 01-Jan-90 -1 ~ :E m 01-Jan-91 -1 "'r---..~ en -t 01-Jan-92 0 t 'TI 01-Jan-93 s: ::u 01-Jan-94 • ru '2. N N O:::c 0) 01-Jan-95 _.1» -. T "I\) 01-Jan-96 CCI\) -0') ""U 01-Jan-97 I» 0-~ ~ C-o 01-Jan-98 ""C 01-Jan-99 -1 ~17 C'" • I\) ~ 01 -Jan-OO ~ J ~! 1 0 0 01-Jan-01 0 ~ 0 01-Jan-02 -1 "1(:IL...L (I) ~ 01 -Jan-03 -1 ~ I" 7'111 ... -.., I» ... 01-Jan-04 -1 ~ .... -o· ~ 01-Jan-05 ~ I :<t::_1 tn • ~ 01-Jan-06 < (I) 01 -Jan-07 -1 ,.. ~ CC (I) ... 01-Jan-08 -1 ~I ____ I I» ... 01-Jan-09 1 I • ~ o· ~ 01-Jan-10 01-Jan-11 01-Jan-12 (Log Scale) a a a a a a a a a 0 0 0 0 0 0 0 0 0 m m m m m m m m m I I I I I I I I + 0 0 0 0 0 0 0 0 0 ex> ....... Q") (]'J ~ VJ '" 0 01-Jan-81 ~ 01-Jan-82 -j I/", I ~ :I: =i 01-Jan-83 -j m s: 01-Jan-84 -j ~I --m en 01-Jan-S5 1 ~ » s: 01-Jan-86 r-r- 01 -Jan-87 en 01-Jan-88 -j I .. I -... 0 C 01-Jan -89 -j I '\... 1_---I. -I :I: 01-Jan-90 -j I. / I --"" ~ m 01-Jan-91 -j /1_"""--1 en -I 01-Jan-92 0 t " 01-Jan-93 s: :::0 r- Q) 01-Jan-94 -r-N ~:;a N 0> 01-Jan-95 _.D) -. T "I\) 01-Jan-96 CCI\) -0') "U 01 -Jan-97 D) c-::::J N C. --" 0 01-Jan-98 "'C C" 01-Jan-99 -j I ;7 17 • I\) ~ 01-Jan-OO -j I ~-0 (') 01-Jan-01 -j _I'" ~ 0 ::::J 01-Jan-02 -j ~~ 0 CD ::::J .... 01-Jan-03 -j .... =-1 ~ .., D) .... 01-Jan-04 -j --I 17 o· ::::J 01-Jan-05 ~ ~ en ::::J 01-Jan-06 < CD 01-Jan-07 -j ~I • I CC CD .... 01-Jan-08 -j /1 .............. I D) .... o· 01-Jan-09 -l ..-== -~ ::::J 01-Jan-10 01-Jan-11 01-Jan-12 ___ . ....l._ WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHEAST OF MILL SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd '82 lS-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nov-82 2nd '83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-84 2nd '85 27-Mar-8S 3rd '8S lS-Jul-8S 4th '8S 09-0ct-8S 2nd '86 24-Mar-86 3rd '86 1O-Jul-86 4th '86 18-0ec-86 2nd '87 20-Apr-87 3rd '87 Os-Jun-87 4th '87 22-0ec-87 2nd '88 19-Apr-88 3rd '88 28-Jul-88 2nd '89 07-Apr-89 3rd '89 06-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd '90 20-Jun-90 3rd '90 17-0ct-90 1st '91 10-Apr-91 2nd '91 ll-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 10-Jun-92 3rd '92 10-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd '93 12-0ct-93 1st '94 ll-May-94 2nd '94 19-Jul-94 3rd '94 28-Nov-94 1st '9S ll-Apr-9S 2nd'9S 06-Jul-9S 3rd '9S lS-Nov-9S 1st '96 23-Apr-96 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd '97 OS-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 OS-Nov-98 2nd '99 ls-Apr-99 3rd '99 07-Jul-99 4th '99 02-0ec-99 2nd '00 21-Apr-00 2nd '00 22-Jun-00 4th '00 21-0ec-00 1st '01 30-Apr-Ol 2nd '01 14-Jun-Ol 4th '01 17-0ec-01 Ra-226 VALUE (uCi/Kg) 3.90E-04 L40E-04 L31E-04 L60E-04 2.67E-06 9.36E-Os L12E-04 L09E-04 3.47E-04 S.61E-04 LOSE-03 8.20E-OS L1SE-04 S.72E-04 S.01E-04 8.70E-04 S.90E-04 L60E-04 2.1OE-04 4.50E-04 3.20E-OS S.60E-04 LSOE-04 6.00E-04 2.60E-04 L80E-04 L60E-04 L20E-04 9.10E-OS 4.S0E-04 3.60E-OS LOOE-OS 7.90E-OS 3.70E-OS 3.00E-Os 6.60E-Os L80E-04 L71E-OS 2.40E-04 6.70E-OS LSOE-OS S.SOE-Os S.20E-OS 3.00E-OS Ll0E-OS Ll0E-OS 8.00E-06 <9.1OE-OS L80E-OS S.70E-OS 2.00E-04 6.03E-OS 2.30E-OS LSOE-04 L20E-06 L60E-06 LOOE-06 2.30E-06 9.10E-06 Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (I.OE-06) 1.0E-OS S.OE-08 Ll0E-03 LOE-04 LOE-06 LOE-OS S.OE-08 6.80E-04 8.0E-OS LOE-06 L3E-OS LOE-06 4.90E-04 7.0E-OS 8.0E-OS LOE-OS S.OE-08 8.00E-04 1.7E-04 LOE-07 L1E-06 LOE-06 L08E-04 9.0E-06 LOE-OS 6.2E-06 8.0E-09 4.97E-04 9.3E-OS LOE-04 L2E-OS 6.0E-06 L84E-04 L2E-OS LOE-06 8.0E-06 4.0E-06 7.80E-04 6.2E-OS 6.0E-OS L2E-OS 2.0E-09 3.7SE-03 L6E-04 4.0E-08 2.0E-04 2.0E-07 7.82E-03 3.3E-04 7.0E-08 3.0E-OS 2.0E-06 3.22E-03 1.4E-04 2.0E-OS 7.0E-06 3.0E-06 7.70E-04 L3E-04 2.0E-04 LOE-OS 3.0E-06 S.10E-04 3.0E-OS 2.0E-OS 2.1E-OS 4.0E-06 2.49E-03 LOE-04 LOE-OS L3E-OS 3.0E-06 LS7E-03 L7E-03 2.0E-04 S.OE-OS 3.0E-06 6.80E-04 3.0E-OS 3.0E-06 7.0E-OS S.OE-08 LSOE-03 LOE-04 LOE-06 3.0E-OS S.OE-08 9.50E-04 4.0E-OS LOE-06 4.0E-OS S.OE-08 L70E-03 1.0E-04 LOE-06 7.0E-OS S.OE-08 L40E-03 LOE-04 LOE-06 2.2E-OS S.OE-08 LSOE-04 4.4E-04 LOE-06 4.0E-OS *** Ll0E-03 LOE-Ol *** 2.0E-OS *** 2.30E-04 2.0E-OS *** S.OE-OS 7.0E-06 2.04E-03 7.0E-OS L4E-OS 3.0E-OS 4.0E-06 3.30E-04 2.0E-OS 2.2E-OS 2.0E-OS S.OE-08 3.20E-04 2.0E-OS LOE-06 2.0E-OS S.OE-08 3.30E-04 2.0E-OS LOE-06 2.0E-OS S.OE-06 3.00E-04 2.0E-OS LOE-06 L6E-OS 2.0E-07 L90E-04 2.0E-OS 2.0E-07 4.0E-OS S.OE-08 L09E-03 S.OE-OS LOE-06 LOE-OS 2.0E-06 LSOE-04 2.0E-OS LOE-OS 7.0E-06 2.0E-07 7.50E-OS 2.0E-OS LOE-06 3.5E-OS 3.0E-06 7.1OE-04 7.0E-OS 2.0E-OS 2.2E-OS 3.0E-06 2.80E-04 3.0E-OS 2.0E-OS loSE-OS 3.0E-06 4.30E-OS 3.5E-OS 2.0E-OS 2.7E-Os 3.0E-06 S.30E-04 6.0E-OS 2.0E-OS 4.0E-OS 3.0E-OS 4.40E-04 6.0E-OS 2.0E-04 L2E-06 9.0E-08 3.00E-OS 6.1E-06 4.5E-06 loSE-OS L7E-07 L70E-04 L1E-OS 8.3E-07 S.4E-06 L6E-07 L40E-04 L3E-OS 7.9E-07 LSE-06 1.5E-07 S.10E-OS 4.5E-06 7.6E-07 S.OE-06 L8E-07 6.70E-OS LOE-OS 8.8E-07 2.SE-06 LSE-07 3.20E-OS 4.SE-06 L8E-07 2.5E-06 L8E-07 L40E-04 7.1E-06 9.3E-07 4.7E-07 L2E-07 4.10E-OS 3.6E-06 6.1E-07 4.3E-07 L3E-07 2.10E-OS 7.3E-07 6.7E-07 L2E~06 S.6E-07 1.40E-04 4.6E-06 L1E-07 9.1E-OS 9.1E-OS <4.50E-04 4.5E-04 4.sE-04 L2E-06 6.3E-08 4.00E-OS L8E-06 3.2E-07 LOE-06 8.2E-08 8.70E-OS S.OE-06 4.1E-07 3.0E-06 L2E-07 3.00E-04 LOE-OS 6.0E-OS 1.4E-06 8.3E-08 L40E-04 4.7E-06 4.2E-07 LOE-06 2.3E-07 2.10E-OS LOE-06 L1E-06 3.0E-06 L2E-07 L60E-04 8.0E-06 S.9E-07 LOE-07 2.8E-07 L60E-04 LOE-OS L4E-06 L1E-06 3.7E-07 S.10E-OS S.OE-06 L9E-06 LOE-07 2.4E-07 <L2E-06 LOE-07 2.4E-07 2.0E-07 9.9E-08 3.80E-06 2.0E-07 S.OE-07 2.4E-06 L2E-07 3.57E-OS 3.0E-06 6.0E-07 1st '02 07-May-02 3.30E-OS LBE-06 7.6E-07 4.50E-OS 2.6E-06 LOE-OS 2nd '02 07-Jul-02 S.5SE-OS 2.BE-06 7.6E-07 S.31E-OS 3.9E-06 LOE-OS 4th '02 lS-0ec-02 7.7SE-OS 3.6E-06 7.6E-07 L29E-04 6.2E-06 LOE-OS 1st '03 21-Mar-03 9.10E-06 L3E-06 3.6E-07 L13E-OS L6E-06 3.4E-06 2nd '03 1O-Jun-03 2.50E-OS L3E-06 3.6E-07 3.26E-06 2.0E-06 7.4E-OB 4th '03 20-Nov-03 S.70E-OS 3.5E-06 1.5E-07 4.0SE-OS S.BE-06 B.3E-07 1st '04 OB-Apr-04 9.3BE-OS 3.7E-06 L1E-07 S.BBE-OS 3.0E-06 S.5E-07 2nd '04 12-Jun-04 S.63E-OS 3.4E-06 LBE-07 6.42E-OS S.9E-06 9.0E-07 4th '04 30-Nov-04 B.41E-OS S.50E-06 2.00E-OB 2.4BE-04 L40E-OS 3.00E-07 1st 'OS 21-Apr-OS S.60E-OS 3.00E-06 L40E-07 S.BOE-OS 4.00E-06 6.90E-07 2nd 'OS 13-Jun-OS 9.10E-06 LSOE-06 LBOE-07 Ll0E-OS L20E-OS 9.00E-07 4th 'OS 10-Nov-OS 6.00E-OS 3.00E-06 LlOE-l0 L70E-06 6.40E-07 S.50E-l0 1st '06 03-Apr-06 B.OOE-OS S.00E-06 S.OOE-OB 3.40E-04 L20E-OS LOOE-06 2nd '06 16-Jun-06 4.lOE-OS 3.lOE-06 S.OOE-OB L16E-04 6.10E-06 LOOE-06 4th '06 2B-Nov-06 L17E-04 4.60E-06 L90E-07 3.2BE-04 9.50E-06 9.S0E-07 1st '07 30-Mar-07 9.70E-OS 4.40E-06 L90E-07 3.40E-04 B.70E-06 B.4-07 2nd '07 l-Jun-07 L30E-OS L60E-06 L90E-07 L20E-04 6.60E-06 9.70E-07 4th '07 23-Nov-07 7.00E-OS B.20E-06 2.00E-07 S.00E-04 2.00E-OS L20E-06 1st 'OB 22-Apr-OB 3.6E-06 3.00E-06 S.20E-07 2.3E-04 1.40E-OS LOOE-06 2nd'OB lB-Jun-OB 3.2E-OS 3.20E-06 1.BOE-06 6.9E-OS 3.S0E-OS S.SOE-OS 4th 'OB 12-0ec-OB 1st '09 2B-Apr-09 S.9E-04 L3SE-OS 1.50E-06 3.4E-04 L30E-OS LSOE-06 2nd '09 17-Jun-09 1.9E-OS L4SE-06 4.90E-07 3.6E-OS Ll0E-OS LBOE-OS 4th '09 lB-Oec-09 L7E-04 S.90E-06 4.BE-04 L20E-OS 1st '10 13-May-lO 2.2E-04 7.20E-06 LlOE-06 L9E-04 L90E-OS 2.90E-OS 2nd '10 lB-Jun-l0 6.5E-OS 3.40E-06 7.60E-07 L4E-04 L90E-OS 2.90E-OS 4th '10 20-0ec-l0 2.3E-OS L70E-06 S.20E-07 LOE-OS LSOE-06 2.30E-06 2nd '11 23-Jun-11 2.4E-07 L4E-07 LBE-07 <2.9E-06 L7E-06 2.9E-06 2nd '12 11-Apr-12 4.4E-OS L9E-06 3.6E-07 2.1E-04 2.0E-06 LOE-06 3rd'12 ll-Jun-12 2.2E-OS B.4E-07 L1E-07 L3E-04 7.6E-06 S.9E-06 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period WHITE MESA MILL FORAGE RADIONUCLIDE DATA NORTHWEST OF MILL SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd '82 lS-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nov-82 2nd '83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-84 2nd '8S 27-Mar-8S 3rd '8S lS-Jul-8S 4th '8S 09-0ct-8S 2nd '86 24-Mar-86 3rd '86 10-Jul-86 4th '86 18-Dec-86 2nd '87 20-Apr-87 3rd '87 OS-Jun-87 4th '87 22-Dec-87 2nd '88 19-Apr-88 3rd '88 28-Jul-88 2nd '89 07-Apr-89 3rd '89 06-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd '90 20-Jun-90 3rd '90 17-0ct-90 1st '91 lO-Apr-91 2nd '91 ll-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 lO-Jun-92 3rd '92 10-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd '93 12-0ct-93 1st '94 ll-May-94 2nd '94 19-Jul-94 3rd '94 28-Nov-94 1st '9S ll-Apr-9S 2nd'9S 06-Jul-9S 3rd '9S lS-Nov-9S 1st '96 23-Apr-96 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd '97 OS-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 OS-Nov-98 2nd '99 lS-Apr-99 3rd '99 07-Jul-99 4th '99 02-Dec-99 2nd '00 21-Apr-00 2nd '00 22-Jun-00 4th '00 21-Dec-00 1st '01 30-Apr-01 2nd '01 14-Jun-01 Ra-226 VALUE (uCi/Kg) 2.73E-03 2.00E-04 L04E-04 2.00E-OS 2.36E-06 8.S8E-OS 1.19E-04 9.78E-OS 2.08E-04 6.0SE-04 L10E-04 6.10E-OS L07E-04 8.86E-04 6.66E-04 S.20E-04 4.10E-04 L60E-04 3.60E-04 2.60E-04 3.10E-OS 6.20E-04 3.40E-04 S.lOE-04 3.60E-04 L70E-04 8.80E-OS 3.00E-04 3.10E-04 S.00E-04 2.00E-OS 6.S0E-06 L20E-04 L80E-OS S.20E-OS S.10E-OS L20E-04 3.73E-OS 2.40E-04 8.40E-OS L90E-OS L20E-04 8.30E-OS 3.60E-OS 3.30E-OS S.40E-06 8.90E-06 <9.20E-OS < 6.S0E-08 4.20E-OS 6.20E-OS S.4SE-OS L10E-04 3.70E-OS 2.90E-OS 2.30E-06 2.10E-OS L30E-06 Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCi/Kg (5.0E-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (1.0E-06) S.OE-OS S.OE-08 7.lOE-03 3.0E-04 LOE-06 LOE-OS S.OE-08 8.30E-04 S.OE-OS LOE-06 9.0E-06 7.0E-06 6.40E-04 S.OE-OS 4.0E-OS LOE-OS S.OE-08 2.20E-04 9.0E-OS LOE-07 9.SE-07 LOE-06 8.00E-OS LOE-OS LOE-OS L4E-OS 2.0E-08 3.53E-04 L9E-OS LOE-OS L1E-OS S.OE-06 LS8E-04 L3E-OS LOE-OS 7.0E-06 2.0E-06 2.16E-03 3.4E-04 3.0E-04 LOE-OS 3.0E-09 1.60E-03 7.0E-OS 3.0E-08 L6E-04 2.0E-07 2.58E-03 L1E-04 3.0E-08 8.0E-06 3.0E-06 8.63E-04 4.2E-OS 3.0E-OS 6.0E-06 2.0E-06 S.40E-04 S.OE-OS S.OE-OS 6.0E-06 2.0E-06 3.80E-04 3.0E-OS 2.0E-OS L8E-OS 2.0E-06 4.40E-03 L9E-04 3.0E-OS L8E-OS 3.0E-06 4.78E-03 2.1E-04 6.0E-OS LOE-04 3.0E-06 L70E-03 LOE-04 6.0E-OS LOE-04 S.OE-08 L60E-03 LOE-04 LOE-06 3.0E-OS S.OE-08 S.5OE-04 4.0E-OS LOE-06 S.OE-OS S.OE-08 1.80E-03 LOE-04 LOE-06 S.OE-OS S.OE-08 L90E-03 LOE-04 LOE-06 L9E-OS S.OE-08 L60E-04 4.0E-OS LOE-06 S.OE-OS *** L70E-03 LOE-04 *** 3.0E-OS *** 7.40E-04 3.0E-OS *** 6.0E-OS 7.0E-06 LOOE-03 7.0E-OS L4E-OS 3.0E-OS 4.0E-06 4.80E-04 2.0E-OS 2.2E-OS 2.0E-OS S.OE-08 3.20E-04 2.0E-OS LOE-06 L6E-OS S.OE-08 2.90E-04 2.0E-OS LOE-06 3.0E-OS S.OE-06 4.10E-04 2.0E-OS LOE-06 3.0E-OS 2.0E-07 4.70E-04 2.0E-OS 2.0E-07 4.0E-OS S.OE-08 LSOE-03 LOE-04 LOE-06 8.0E-06 2.0E-06 9.60E-OS L4E-OS LOE-OS 6.0E-06 2.0E-06 L20E-04 2.0E-OS LOE-06 4.0E-OS 3.0E-06 L21E-03 8.0E-OS 2.0E-OS L7E-OS 3.0E-06 2.10E-04 3.0E-OS 2.0E-OS L9E-OS 3.0E-06 L70E-OS 3.6E-OS 2.0E-OS 2.3E-OS 3.0E-06 7.10E-04 6.0E-OS 2.0E-OS LOE-OS 3.0E-OS 9.80E-04 L6E-04 2.0E-04 L6E-06 8.4E-08 7.80E-OS 7.1E-06 4.2E-07 loSE-OS L7E-07 2.60E-04 L3E-OS 8.3E-07 6.1E-06 LSE-07 L20E-04 L1E-OS 7.SE-OS 1.5E-06 L4E-07 4.50E-OS 4.3E-06 7.2E-07 6.8E-06 L4E-07 LOOE-OS S.8E-06 7.1E-07 3.3E-06 L9E-07 6.80E-OS 6.3E-06 L8E-07 2.5E-06 L6E-07 8.S0E-OS S.6E-06 8.4E-07 2.3E-06 L7E-07 4.40E-OS 4.8E-06 8.4E-07 3.5E-07 1.6E-07 3.20E-OS 9.0E-07 7.8E-07 7.2E-07 S.4E-07 3.40E-04 6.7E-06 L1E-07 9.2E-OS 9.2E-OS <4.60E-04 4.6E-04 4.6E-04 6.SE-08 6.5E-08 <3.20E-07 3.2E-07 3.2E-07 LOE-06 L1E-07 L70E-04 LOE-OS S.5E-07 LOE-06 LOE-07 1.40E-04 7.0E-06 LOE-07 L4E-06 8.3E-08 9.20E-OS 4.0E-06 4.2E-07 3.0E-06 2.2E-07 2.80E-OS LOE-06 L1E-06 LOE-06 2.4E-07 2.70E-04 LOE-OS L2E-06 LOE-06 3.3E-07 2.80E-04 2.0E-OS L7E-06 L4E-06 3.7E-07 3.30E-04 S.OE-OS L9E-06 LOE-06 LSE-07 <7.6E-07 N/A 7.6E-07 4.0E-08 L2E-07 L80E-06 3.0E-08 S.9E-07 4th '01 17-0ec-Ol 3.70E-Os 7.67E-07 8.30E-08 6.72E-Os 2.62E-06 6.00E-07 1st '02 07-May-02 4.90E-Os 2.40E-06 7.60E-07 L28E-04 s.61E-06 LOOE-Os 2nd '02 07-Jul-02 8.88E-Os 4.32E-06 7.60E-07 8.33E-Os 4.32E-06 LOOE-Os 4th '02 ls-0ec-02 LsOE-04 6.2E-06 7.60E-07 3.16E-04 L07E-Os LOE-Os 1st '03 21-Mar-03 s.OOE-Os 3.4E-06 2.71E-06 <4.2e-6 4.20E-06 2nd '03 10-Jun-03 s.60E-Os 2.0E-06 4.lOE-07 L88E-04 s.14E-06 8.2E-08 4th '03 20-Nov-03 3.20E-04 8.2E-06 L70E-07 4.89E-04 L2sE-Os 8.3E-07 1st '04 08-Apr-04 6.29E-Os 4.1E-06 2.00E-07 L94E-Os 4.00E-06 LOE-06 2nd '04 12-Jun-04 6.s1E-Os 3.4E-06 L30E-07 L87E-Os 3.90E-06 6.5E-07 4th '04 30-Nov-04 7.s0E-Os 4.6E-06 2.0E-08 4.4sE-04 L40E-Os 3.0E-07 1st 'OS 21-Apr-Os 4.90E-Os 2.70E-06 L30E-07 L27E-04 4.80E-06 6.50E-07 2nd 'OS 13-Jun-Os 2.30E-Os 2.10E-06 LsOE-07 4.70E-Os s.10E-06 7.60E-07 4th 'OS 10-Nov-Os 7.40E-Os 3.50E-06 L20E-l0 2.40E-06 8.10E-08 s.80E-l0 1st '06 03-Apr-06 LOOE-04 6.00E-06 s.00E-08 6.s4E-04 LsOE-Os LOOE-06 2nd '06 16-Jun-06 9.s0E-Os s.90E-06 s.00E-08 4.48E-04 L40E-Os LOOE-06 4th '06 28-Nov-06 8.13E-Os 4.10E-06 2.20E-07 3.2sE-04 L12E-06 LOOE-Os 1st '07 30-Mar-07 4.30E-Os 2.60E-06 L70E-07 2.64E-04 7.20E-06 8.60E-07 2nd '07 l-Jun-07 s.10E-Os 3.20E-06 2.30E-07 s.30E-04 L40E-06 L20E-06 4th '07 23-Nov-07 7.30E-Os 6.6E-06 s.OE-08 7.00E-04 2.20E-Os 1.10E-06 1st '08 22-Apr-08 2.8E-06 2.8E-06 7.20E-07 4.40E-04 2.0E-Os LOE-06 2nd '08 18-Jun-08 3.2E-06 3.3E-06 L80E-06 1.40E-04 3.3E-Os s.5E-Os 4th '08 12-0ec-08 7.3E-Os 3.2E-06 7.40E-07 4.40E-04 2.5E-Os 3.2E-Os 1st '09 28-Apr-09 s.3E-Os 3.6E-06 Ll0E-06 L90E-04 loSE-OS 2.2E-Os 2nd '09 17-Jun-09 2.3E-Os L6E-Os s.2E-07 4.30E-Os LOOE-Os L7E-Os 4th '09 18-0ec-09 s.sOE-Os 3.s0E-06 3.0E-04 Ll0E-Os 1st '10 13-May-10 L9E-04 6.lOE-06 9.40E-07 s.lE-04 2.40E-Os 3.10E-Os 2nd '10 18-Jun-1O 2.3E-Os 2.00E-06 7.70E-07 8.3E-Os L80E-Os 2.90E-Os 4TH '10 20-0ec-l0 8.6E-06 9.10E-07 3.90E-07 L1E-07 6.80E-07 Ll0E-06 2nd '11 23-Jun-11 2.1E-07 L20E-07 L40E-07 <2.2E-06 L30E-06 2.20E-06 2nd '12 11-Apr-12 loSE-OS 9.50E-07 2.60E-07 <7.0E-07 6.00E-07 LOOE-06 3rd'12 11-Jun-12 8.3E-06 s.40E-07 L20E-07 L4E-04 8.30E-06 6.50E-06 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period WHITE MESA MILL FORAGE RADIONUCLIDE DATA SOUTHWEST OF MILL SAMPLED QTR. SAMPLED DATE 3rd '81 27-Aug-81 4th '81 20-0ct-81 2nd '82 lS-Apr-82 3rd '82 01-Jul-82 4th '82 30-Nov-82 2nd '83 13-Apr-83 3rd '83 01-Jul-83 4th '83 30-Jan-84 2nd '84 28-Jun-84 4th '84 14-Nov-84 2nd'8S 27-Mar-8S 3rd '8S lS-Jul-8S 4th '8S 09-0ct-8S 2nd '86 24-Mar-86 3rd '86 10-Jul-86 4th '86 18-Dec-86 2nd '87 20-Apr-87 3rd '87 OS-Jun-87 4th '87 22-Dec-87 2nd '88 19-Apr-88 3rd '88 28-Jul-88 2nd '89 07-Apr-89 3rd '89 06-Jun-89 4th '89 07-Nov-89 1st '90 17-Apr-90 2nd '90 20-Jun-90 3rd '90 17-0ct-90 1st '91 10-Apr-91 2nd '91 ll-Jun-91 3rd '91 20-Nov-91 1st '92 22-Apr-92 2nd '92 10-Jun-92 3rd '92 10-Jun-92 1st '93 13-Apr-93 2nd '93 26-Jun-93 3rd '93 12-0ct-93 1st '94 ll-May-94 2nd '94 19-Jul-94 3rd '94 28-Nov-94 1st '9S ll-Apr-9S 2nd '9S 06-Jul-9S 3rd '9S lS-Nov-9S 1st '96 23-Apr-96 2nd '96 * 31-Jul-96 3rd '96 14-Nov-96 1st '97 21-Apr-97 3rd '97 OS-Sep-97 4th '97 20-Nov-97 1st '98 23-Mar-98 2nd '98 16-Jun-98 4th '98 OS-Nov-98 2nd '99 lS-Apr-99 3rd '99 07-Jul-99 4th '99 02-Dec-99 2nd '00 21-Apr-00 2nd '00 22-Jun-00 4th '00 21-Dec-00 1st '01 30-Apr-01 2nd '01 14-Jun-01 Ra-226 VALUE (uCi/Kg) 9.S0E-04 3.00E-OS 1.37E-OS 3.40E-04 1.7SE-OS 7.13E-04 S.39E-OS 6.40E-OS 8.27E-OS 2.72E-04 4.73E-04 6.60E-OS 2.83E-04 1.57E-04 3.78E-04 2.60E-04 4.1DE-04 2.90E-04 1.80E-04 2.30E-04 1.S0E-04 3.1DE-04 1.30E-04 4.30E-04 2.50E-04 1.10E-04 6.10E-OS 3.40E-OS 8.00E-OS 6.S0E-OS 1.60E-OS 1.90E-OS 1.60E-OS 2.60E-OS 3.00E-OS 3.1DE-OS 2.00E-OS 1.7SE-OS 1.00E-04 1.70E-OS 6.40E-06 2.30E-OS 4.20E-OS 2.1DE-OS S.50E-06 S.30E-06 2.50E-OS <7.90E-OS 3.60E-07 4.30E-OS 2.40E-OS 2.23E-OS 1.S0E-04 1.00E-04 1.30E-06 1.20E-06 1.80E-06 2.60E-06 Ra-226 LLD Pb-210 Pb-210 LLD ERROR (uCi/Kg) uCi/Kg (S.OE-08) VALUE (uCi/Kg) ERROR (uCi/Kg) uCi/Kg (1.OE-06) 2.0E-OS S.OE-08 1.S0E-04 1.0E-OS 1.0E-06 3.0E-06 S.OE-08 1.S0E-04 2.0E-OS 1.0E-06 3.0E-06 3.0E-06 3.80E-04 4.0E-OS 4.0E-OS 2.0E-OS S.OE-08 3.68E-03 2.7E-04 1.0E-07 3.0E-06 2.0E-06 7.92E-04 4.0E-06 2.0E-OS 7.3E-OS 9.0E-08 2.S1E-03 3.0E-04 3.0E-04 4.5E-06 2.0E-06 6.88E-04 4.3E-OS 4.0E-OS 7.0E-06 4.0E-06 1.20E-03 1.0E-04 4.0E-OS 6.3E-06 3.0E-09 1.80E-03 1.0E-04 9.0E-08 1.SE-04 2.0E-07 4.70E-03 7.2E-04 3.0E-07 1.6E-07 3.OE-06 7.07E-04 3.6E-OS 3.0E-OS 7.0E-06 4.0E-06 4.90E-04 3.0E-OS 3.0E-OS 2.0E-OS 7.0E-06 1.S0E-03 1.0E-04 7.0E-OS 1.0E-OS 4.0E-06 4.14E-03 1.8E-04 3.0E-OS 1.0E-OS 2.0E-06 1.6SE-02 7.0E-04 1.0E-04 2.0E-OS 2.0E-06 1.70E-03 1.0E-04 1.0E-04 7.0E-OS S.OE-08 2.20E-03 1.0E-04 1.0E-06 4.0E-OS S.OE-08 7.S0E-04 S.OE-OS 1.0E-06 3.0E-OS S.OE-08 2.40E-03 1.0E-04 1.0E-06 S.OE-OS S.OE-08 2.90E-03 1.0E-04 1.0E-06 3.0E-OS S.OE-08 4.30E-03 2.0E-04 1.0E-06 4.0E-OS *** 4.20E-03 1.0E-04 *** 2.0E-OS *** 1.S0E-03 1.0E-04 *** S.OE-OS 1.4E-OS 3.S0E-03 1.4E-04 2.7E-OS 3.0E-OS S.OE-06 2.39E-03 S.OE-OS 2.5E-OS 2.0E-OS S.OE-08 6.60E-04 3.0E-OS 1.0E-06 l.4E-OS S.OE-08 6.10E-04 3.0E-OS 1.0E-06 1.1E-OS S.OE-06 2.20E-04 1.0E-OS 1.0E-06 6.0E-06 2.0E-07 1.20E-04 1.0E-OS 2.0E-07 1.4E-OS S.OE-08 9.10E-04 S.OE-OS 1.0E-06 7.0E-06 2.0E-06 3.20E-04 2.0E-OS 1.0E-OS 1.0E-OS 2.0E-07 2.20E-04 2.0E-OS 1.0E-06 1.8E-OS 3.OE-06 7.60E-04 6.0E-OS 2.0E-OS 2.0E-OS 3.0E-06 3.40E-04 3.0E-OS 2.0E-OS l.4E-OS 3.0E-06 O.OOE+OO 3.0E-OS 2.0E-OS 1.6E-OS 3.0E-06 4.20E-04 6.0E-OS 2.0E-OS S.OE-06 3.OE-OS 3.90E-04 8.0E-OS 2.0E-04 1.7E-06 7.6E-08 1.30E-04 7.8E-06 3.8E-07 9.0E-06 1.SE-07 2.60E-04 1.2E-OS 7.4E-07 1.SE-06 1.6E-07 1.60E-04 1.SE-OS 8.1E-07 6.0E-07 1.4E-07 4.40E-OS 4.2E-06 7.0E-07 2.2E-06 1.7E-07 6.60E-OS 9.6E-06 8.3E-07 2.2E-06 1.7E-07 1.00E-04 6.7E-06 1.8E-07 2.0E-06 1.6E-07 1.90E-04 7.3E-06 8.2E-07 4.2E-07 1.4E-07 3.30E-OS 3.9E-06 7.0E-07 3.2E-07 1.3E-07 1.90E-OS 6.9E-07 6.3E-07 9.SE-07 S.9E-07 1.30E-04 4.7E-06 1.2E-07 7.9E-OS 7.9E-OS <3.90E-04 3.9E-04 3.9E-04 1.4E-07 3.3E-08 <1.7E-07 1.7E-07 1.7E-07 1.0E-06 7.6E-08 2.S0E-04 1.0E-OS 3.8E-07 1.0E-06 1.2E-07 1.70E-04 8.0E-06 6.2E-07 8.6E-07 1.2E-07 2.30E-04 7.0E-06 S.9E-07 3.0E-06 2.0E-07 1.70E-OS 1.0E-06 1.0E-06 2.0E-06 1.2E-07 1.1DE-04 7.0E-06 6.1E-07 1.0E-07 2.4E-07 2.00E-04 1.0E-OS 1.2E-06 9.0E-07 2.4E-07 1.20E-04 3.0E-OS 1.2E-06 1.0E-07 1.7E-07 <8.3E-07 N/A 8.3E-07 2.0E-07 9.9E-08 1.1DE-06 2.0E-08 S.OE-07 4th '01 17-Dec-Ol 2.63E-06 4.6E-OS L2E-07 9.40E-OS 3.7E-06 6.0E-07 1st '02 07-May-02 3.50E-OS 2.2E-06 7.6E-07 L36E-04 S.6E-06 LOE-OS 2nd '02 07-Jul-02 4.02E-OS 2.3E-06 7.6E-07 7.04E-OS 4.1E-06 LOE-OS 4th '02 lS-Dec-02 B.l0E-OS 3.9E-06 7.6E-07 2.B7E-04 B.SE-06 LOE-OS 1st '03 21-Mar-03 3.70E-OS 2.6E-06 2.4E-06 2.69E-OS 2.0E-06 3.7E-06 2nd '03 lO-Jun-03 L30E-OS LOE-06 S.2E-07 <LOOE-07 LOE-07 4th '03 20-Nov-03 L60E-04 L3E-OS L2E-07 L42E-04 6.4E-06 S.9E-07 1st '04 OB-Apr-04 L40E-04 7.7E-06 1.lE-07 6.10E-06 2.7E-06 S.5E-07 2nd '04 12-Jun-04 6.51E-OS 3.2E-06 1.5E-07 S.27E-OS 4.9E-06 7.6E-07 4th '04 30-Nov-04 B.40E-OS S.7E-06 3.0E-OB 3.39E-04 L6E-OS 3.0E-07 1st 'OS 21-Apr-OS L70E-OS L6E-06 L3E-07 4.S0E-OS 3.5E-06 6.5E-07 2nd 'OS 13-Jun-OS LSOE-OS L6E-06 L4E-07 7.00E-OS S.lE-06 6.9E-07 4th 'OS lO-Nov-OS 3.BOE-OS 2.1E-06 B.6E-lO L20E-06 4.BE-OB 4.3E-lO 1st '06 03-Apr-06 LOOE-04 6.0E-06 S.OE-OB 3.30E-04 L1E-OS LOE-06 2nd '06 16-Jun-06 3.40E-OS 2.5E-06 S.OE-OB L37E-04 6.0E-06 LOE-06 4th '06 2B-Nov-06 7.31E-OS 3.20E-06 L60E-07 2.9BE-04 B.SOE-06 B.20E-07 1st '07 30-Mar-07 3.00E-OS 2.20E-06 L70E-07 3.20E-04 7.90E-06 B.40E-07 2nd '07 l-Jun-07 LlOE-04 4.60E-06 2.3-07 3.20E-04 LlOE-OS Ll0E-06 4th '07 23-Nov-07 S.60E-OS S.20E-06 S.OOE-OB 6.40E-04 L90E-OS LOOE-06 1st 'OB 22-Apr-OB 3.20E-OS 2.30E-06 7.20E-07 2.30E-04 LSOE-OS LOOE-06 2nd'OB lB-Jun-OB L2SE-OS 2.20E-06 LBOE-06 S.OOE-OS 3.00E-OS 4.BOE-03 4th 'OB 12-Dec-OB 1st '09 2B-Apr-09 2.60E-OS 2.90E-06 L40E-06 3.70E-OS LSOE-06 2.50E-OS 2nd '09 17-Jun-09 2.40E-OS 1.40E-06 3.90E-07 3.50E-OS 7.90E-06 L30E-OS 4th '09 lB-Dec-09 3.1E-OS 2.30E-06 2.1E-04 B.40E-06 1st '10 13-May-l0 2.0E-OS 2.10E-06 9.40E-07 S.6E-OS LSOE-OS 2.40E-OS 2nd'lO lB-Jun-lO L1E-OS 1.30E-06 6.60E-07 7.BE-OS L60E-OS 2.50E-OS 4th '10 20-Dec-lO 6.7E-06 9.10E-07 4.BOE-07 B.OE-07 7.90E-07 L30E-06 2nd '11 23-Jun-11 <L7E-07 6.9E-OB L7E-07 <2.5E-06 1.5E-06 2.5E-06 2nd '12 11-Apr-12 S.OE-06 6.0E-07 3.0E-07 <7.0E-07 7.0E-07 LOE-06 3rd'12 11-Jun-12 L9E-OB 6.2E-OB L1E-07 <2.5E-07 L3E-06 2.2E-06 *2nd quarter of 1996 San Juan County, Utah, was declared a disaster area due to drought, no samples were collected during this period Er\ERGY LABORATORIES wWw.energylab.com Anatytic81 Exti1JJBJiC. Sincs 7152 -~,~-[~Qa/Mfil-~~(t2roill .:Bimngs. Ml800-135-44B9 . C~spef,WV 888-235-0$15 ~) ~,ilSil(6,:JjJj ·~ap.id c'ity;$~88~-&12-12~.5 • CQllege Station, "IX S,8 .. SQO-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp Early Spring Vegetation 2012 C 12040818-00 1 Client Sample 10: North East Analyses RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC lead 210 altu lead 210 precision (±) altu lead 210 MOC altu Radium 226 Radium 226 precision (±) Radium 226 MOC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 2.1 E-04 2.0E-06 1.0E-06 217 2 4.4E-05 1.9E-06 3.6E-07 44 1.9 0.36 MOC -Minimum detectable concentration Units uCi/kg uCi/kg uCi/kg pCi/kg pCi/kg pCi/kg uCi/kg uCi/kg uCi/kg pCi/kg pCi/kg pCi/kg Qualifier RL Report Date: 06/05/12 Collection Date: 04/11/1209:00 DateReceived: 04/16/12 Matrix: Vegetation MCL! QCL Method Analysis Date 1 By E909.0 05122/12 11 :041 eli-cs E909.0 05122/12 11 :04 1 eli-cs E909.0 05122112 11 :04 1 eli-cs E909.0 05122/12 11 :04 1 eli-cs E909.0 05122/12 11 :04 1 eli-cs E909.0 05122112 11 :041 eli-cs E903.0 05/10/12 15:591 trs E903.0 0511 0112 15 :59 1 trs E903.0 05/10/12 15:591 trs E903.0 05/10/12 15:591 trs E903.0 05/10/12 15:591 trs E903.0 0511 0112 15 :59 1 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 30f9 Ef\ERGY LABORATORiES www.energyJab.com AIiBIytitaI ExcsJfSIICB Sines' 152 _ Helena, MT 877;.472-0711 • Billings, MT BOO-735-4489 • Casper, W'f 888-235-0515 'mll~tte;'WY'66:-6B6-7175 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project : Lab ID: Denison Mines USA Corp Late Spring Vegetation 2012 C12060622-001 Client Sample ID: North East Analyses RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC lead 210 altu lead 210 precision (±) altu lead 210 MOC altu Radium 226 Radium 226 precision (±) Radium 226 MOC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 1.3E-04 7.6E-06 5.9E-06 132 7.6 5.9 2.2E-05 8.4E-07 1.1 E-07 21.8 0.84 0.11 MOC - Minimum detectable concentration Units uCi/kg uCi/kg uCi/kg pCi/kg pCi/kg pCi/kg uCi/kg uCi/kg uCi/kg pCi/kg pCi/kg pCi/kg Qualifier Rl Report Date: 08/09/12 Collection Date: 06/11/12 13 :00 DateReceived: 06/14/12 Matrix: Vegetation MCL! QCl Method Analysis Date 1 By E909.0 07130/12 23:51 1 eli-cs E909.0 07/30/1223:51 1 eli-cs E909.0 07130/12 23:51 1 eli-cs E909.0 07130/12 23:51 1 eli-cs E909.0 07/30/1223:51 1 eli-cs E909.0 07130/12 23:51 1 eli-cs E903.0 07117/12 01 :441 trs E903.0 07/17/1201 :44 1 trs E903.0 07117/12 01 :44 1 trs E903.0 07117/12 01 :44 1 trs E903.0 07/17/1201 :44 1 trs E903.0 07117/12 01 :44 1 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 9 EI'.ERGY LABORATORI ES www.energylab.com A/la1ytita1£xcBDBfICi Sines 1152 , ' }~ei~Mt";,MtB~1;~4l~~011l .BillillgS, MY 800 .. r35-44~9 • Casper, W'f 888-235-0~15 §!1I~lte.J ~;8§c6:'QBJ~111~ ·R"@p'i~ Cijy"S~ 88'-672~1225 • CollegeStat!on, ti 888~6'O-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp Early Spring Vegetation 2012 C 1204081 8-002 Client Sample ID: North West Analyses RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC lead 210 altu lead 210 precision (±) altu lead 210 MOC altu Radium 226 Radium 226 precision (±) Radium 226 MOC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result -7.0E-07 6.0E-07 1.0E-06 -0.7 0.6 1.5E-05 9.5E-07 2.6E-07 15 0.95 0.26 MOC -Minimum detectable concentration Units uCi/kg uCilkg uCi/kg pCi/kg pCi/kg pCilkg uCi/kg uCi/kg uCi/kg pCi/kg pCi/kg pCi/kg Report Date: 06/05/12 Collection Date: 04/11/12 10:00 DateReceived: 04/16/12 Matrix: Vegetation MCL! Qualifier Rl QCl Method Analysis Date 1 By U E909.0 05122/12 16:09 1 eli-cs E909.0 05/22/12 16:091 eli-cs E909.0 05122/12 16:091 eli-cs U E909.0 05/22/1216:091 eli-cs E909.0 05/22/1216:091 eli-cs E909.0 05/22/12 16:091 eli-cs E903.0 05/10/12 15:591 trs E903.0 05/10/12 15:591 trs E903.0 0511 0112 15 :59 1 trs E903.0 05/10/12 15:591 trs E903.0 05/10/12 15:591 trs E903.0 05/10/12 15:591 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 4 of9 C'tl www.energylab.com i ;"" ... , Hel'na, MT 817·472-0711 • Billings, MT 800.135-4489 • Casper, WY B88·23H515 . ~,,::.:, Anafytii:aIExC8llBIICIlSincB'952 ~.ui~~,,~'~n,le.#~,wY:Q66 .. &.86-7n5 • Rapi~ City, SO 888-672-1225 • College Station, IX 888-690-2218 EN:RGY LABORATORIES LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp Late Spring Vegetation 2012 C 12060622-002 Client Sample ID: North West Analyses RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC lead 210 altu lead 210 precision (±) altu lead 210 MOC altu Radium 226 Radium 226 precision (±) Radium 226 MOC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 1.4E-04 8.3E-06 6.5E-06 138 8.3 6.5 8.3E-06 5.4E-07 1.2E-07 8.3 0.54 0.12 MOC -Minimum detectable concentration Units uCi/kg uCi/kg uCi/kg pCilkg pCi/kg pCi/kg uCi/kg uCi/kg uCilkg pCi/kg pCi/kg pCi/kg Qualifier RL Report Date: 08/09/12 Collection Date: 06/11/12 12:15 DateReceived: 06/14/12 Matrix: Vegetation MCL! QCL Method Analysis Date / By E909.0 07/31/1202:141 eli-cs E909.0 07/31/1202:141 eli-cs E909.0 07/31/1202:141 eli-cs E909.0 07/31/1202:141 eli-cs E909.0 07/31/1202:141 eli-cs E909.0 07/31/1202:141 eli-cs E903.0 07117/12 01 :44 1 trs E903.0 07/17/1201 :44 1 trs E903.0 07/17/1201 :44 1 trs E903.0 07117/12 01 :441 trs E903.0 07117/12 01 :44 1 trs E903.0 07117/12 01 :44 1 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of9 EI\ERGY LABORAT ORIES www.imergylab.com AnaIYlitBI Ext8JJenc1. SiiICS 1952 Hei~"1J~ (,["~~J~41:~,~0711 e Billings,MT 800~135~44B9 • Casper, WYa88~235-0515 . Gi1!!@~ wr~t6§~Jj§"lj,'1:~ ~~c!Pi·dCitY,$D.,'888,:&12~:12~5 • ColleglrStat!on, TX 888-6QO-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp Early Spring Vegetation 2012 C 12040818-003 Client Sample ID: South West Analyses RADIONUCLIDES -TOTAL lead 210 lead 210 precision (±) lead 210 MOC lead 210 altu lead 210 precision (±) altu lead 210 MOC altu Radium 226 Radium 226 precision (±) Radium 226 MOC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOC Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result -?OE-O? ?OE-O? 1.0E-06 -O.? O.? 5.0E-06 6.0E-0? 3.0E-0? 5.0 0.60 0.30 MOC -Minimum detectable concentration Units uCi/kg uCilkg uCi/kg pCi/kg pCi/kg pCilkg uCi/kg uCi/kg uCi/kg pCi/kg pCilkg pCi/kg Report Date: 06/05/12 Collection Date: 04/11/12 12:00 DateReceived: 04/16/12 Matrix: Vegetation MCL! Qualifier RL QCL Method Analysis Date 1 By U E909.0 05122/12 21 :141 eli-cs E909.0 05/22/12 21 : 14 1 eli-cs E909.0 05122/12 21 :14 1 eli-cs U E909.0 05122112 21 :14 1 eli-cs E909.0 05122/12 21 :14 1 eli-cs E909.0 05/22112 21 : 14 1 eli-cs E903.0 05/10/12 15:591 trs E903.0 05/10/12 15:59 1 trs E903.0 05/10/12 15:591 trs E903.0 05/10/12 15:591 trs E903.0 05/1 0112 15 :59 1 trs E903.0 05/10/12 15:59 1 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 50f9 EN:RGY LABORATORiES www.energylab.com Analytical ExcsllwB Sincs 7852 Helena, MT 877~472-0711 • Billings, MT 800-735~4489 . Casper, WV 888-235-0515 ,~UI~tte, wY ,86&·6B6 .. 7115 • Rapid City, SD 888-672-1225 • College Station, IX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp Late Spring Vegetation 2012 C 1 2060622-003 Client Sample ID: South West Analyses RADIONUCLIDES lead 210 lead 210 precision (±) lead 210 MOC lead 210 altu lead 210 precision (±) altu lead 210 MOC altu Radium 226 Radium 226 precision (±) Radium 226 MOC Radium 226 altu Radium 226 altu precision (±) Radium 226 altu MOC -See Case Narrative regarding Pb210 analysis. Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result -2.5E-07 1.3E-06 2.2E-06 -0.25 1.3 2.2 1.9E-08 6.2E-08 1.1 E-07 0.019 0.062 0.11 MOC -Minimum detectable concentration Units uCi/kg uCi/kg uCi/kg pCi/kg pCi/kg pCi/kg uCi/kg uCi/kg uCi/kg pCi/kg pCilkg pCi/kg Report Date: 08/09/12 Collection Date: 06/11/12 13:30 DateReceived: 06/14/12 Matrix: Vegetation MCL! Qualifier RL QCL Method Analysis Date / By U E909.0 08102/12 22:11 1 eli-cs E909.0 08102/12 22:11 1 eli-cs E909.0 08102112 22:11 1 eli-cs U E909.0 08102/12 22:11 1 eli-cs E909.0 08102/12 22:11 1 eli-cs E909.0 08102/12 22:11 1 eli-cs U E903.0 07117/12 01 :44 1 trs E903.0 07117/12 01 :44 1 trs E903.0 07117/12 01 :44 1 trs U E903.0 07117/12 01 :44 1 trs E903.0 07/17/12 01 :441 trs E903.0 07117/12 01 :44 1 trs MCl -Maximum contaminant level. NO -Not detected at the reporting limit. U -Not detected at minimum detectable concentration Page 50f9 Er\ERGY LABORATORIES June os, 2012 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 wWw.energylab.com Analytitaf Extsnenc;. Sines 1952 ANALYTICAL SUMMARY REPORT Workorder No.: C12040818 Project Name: Early Spring Vegetation 2012 Energy Laboratories, Inc. Casper WY received the following 3 samples for Denison Mines USA Corp on 4/16/2012 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C 12040818-00 1 North East 04/11/12 9:00 04/16/12 Vegetation Digestion, Radiochemistry Lead 210 Radium 226 ---------------*-----*---_._------------- C 12040818-002 North West 04/11/12 10:00 04/16/12 Vegetation Same As Above C 12040818-003 South West 04/11/12 12:00 04/16/12 Vegetation Same As Above The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. Data corrected for moisture content are typically noted as - dry on the report. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. If you have any questions regarding these test results, please call. Report Approved By: cS¥~D uJ~~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.06.05 10:38:09 -06:00 Page 1 of 9 wWw.eri~rgylab.CBm AnsljjltllEtUklJ ~ 1952 CLIENT: Denison Mines USA Corp Project: Early Spring Vegetation 2012 Sample Delivery Group: C12040818 BRANCH LABORATORY SUBCONTRACT ANALYSIS Report Date: 06/05/12 CASE NARRATIVE Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520 ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Virginia: 00057; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of9 Ef\ERGY LABORATORIES wWw.energyJab.com ARaljlitafExcSlIsncs Sinis 1852 :";~le'1a, MI'IU'-'(1270ni • Billings, MT 800-735-4489 • Casper, wy 888-235-0515 ~6~!~_i:lill .:R~p.i~<GitY!S~,8.8:-672~12t5 . ColI~ge Station, IX 888"6QO-~218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Early Spring Vegetation 2012 Analyte Count Result Units Method: E903.0 Sample 10: C12040818-001AMS Radium 226 Sample 10: C12040818-001AMSO Radium 226 Sample 10: MB-33509 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: LCS-33509 Radium 226 Qualifiers: RL -Analyte reporting limit. 3 MOC -Minimum detectable concentration Sample Matrix Spike 5.9E-05 uCi/kg Sample Matrix Spike Duplicate 6.0E-05 uCilkg Method Blank 1 E-07 uCi/kg 1E-07 uCi/kg 3E-07 uCi/kg Laboratory Control Sample 1.0E-05 uCi/kg Report Date: 06/05/12 Work Order: C12040818 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: BERTHOLD 770-2_120502B 90 70 130 Run: BERTHOLD 770-2_120502B 97 70 130 1.9 Run: BERTHOLD 770-2_120502B Run: BERTHOLD 770-2_120502B 82 70 130 NO -Not detected at the reporting limit. Batch: RA226-5973 05/10/12 15:59 05/10/12 15:59 17.3 05/10/12 15:59 U 05/10/12 20:58 U -Not detected at minimum detectable concentration Page 6 of 9 EN:RGY LABORATORIES wWii.energylab.com Anlt;tiI;al£XcmJsncdi1Jcs 1952 , ~~fel1~' ~r-8l1~12,:0711 • Billings, MT 800-735-4489 • Casper, W'f 888-235-0~15 Gjll~te, W'(-iH .. j~6:1J?§·R,~Ri(City, SI).88B~.t2-1225 • c~lIegeStation, TX 888-&90-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Early Spring Vegetation 2012 Analyte Method: E909.0 Sample 10: MB-16263 Lead 210 Lead 210 precision (±) Lead 210 MDC Sample 10: LCS-16263 Lead 210 Sample 10: C12040818-003AMS Lead 210 Sample 10: C12040818-003AMSO Lead 210 Count Result Units 3 Method Blank 3E-06 uCi/kg 3E-06 uCi/kg 4E-06 uCi/kg Laboratory Control Sample 0.00053 uCi/kg Sample Matrix Spike 0.00047 uCilkg Sample Matrix Spike Duplicate 0.00046 uCi/kg Report Date: 06/05/12 Work Order: C12040818 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: SUB-T45518 Run: SUB-T45518 95 70 Run: SUB-T45518 105 70 Run: SUB-T45518 103 70 130 130 130 1.6 Batch: T _16263 05/22/12 00:54 U 05/22/12 05:59 05/23/1202:19 05/23/12 07:24 12.2 ._---------------------------- Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. MDC -Minimum detectable concentration U -Not detected at minimum detectable concentration Page 7of9 EN:RGY LABORATORIES ~,,; .www.energylab.com ~ AnalytIcal ExUHBIICI Sine, '952 Workorder Receipt Checklist Denison Mines USA Corp Login completed by: Kristy Gisse Reviewed by: BL2000\kschroeder Reviewed Date: 4/17/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) Container/Temp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 1{1 Yes 1{1 Yes D Yes 1{1 Yes 1{1 Yes 1{1 Yes 1{1 Yes 1{1 Yes 1{1 Yes 1{1 N/A"C Yes D Yes D 1111111111111 il~ 1111111111 ~IIIIIIIIIIII C12040818 Date Received: 4/16/2012 Received by: kg No D No D No D No D No D No D No D No D No D No D No D No D Carrier Ground name: Not Present D Not Present D Not Present 1{1 No VOA vials submitted 1{1 Not Applicable 1{1 Page 8 of 9 TR#l-r9Y Chain of Custody and Analytical Request Record Page -L of ---1.-•• ,nJl'JIlli.»JJ.iLW PLEASE PRINT (Provide as much information as possible.) Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: DeA;SDA M -j A.."''s: £,()...rty .spr-iV\.~ V~~ -t~\-'Ov\. ~\, State: V""" Yes 1St No 0 Report Mail Address: Po 50 y. gOq Contact Name: Phone/Fax: Email: Sampler: (Please Print) 81o..~J..~~~ gYSlt 6~r'-I'" P~l;4l\~ '-135 .' ( 2.2.:2.\ Go.rri t.Ao. P"'\MGr vi Invoice Address: Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: So..~ 5~~ Special Report/Formats: ~[S W@U@ oorn®([J~§[ID • Contact Ell prior to -Shtpp8CJDy: ~ 4.f':?"~ CI "-RUSH sample submittal ~o Ul~ ...-for charges and Cooler ID(s): ~m;,g51 tD 0 ~ R scheduling -See I J.enf .-> 0 >-a; UJ t:.. I nstruction Page Dow o EDD/EDT(Electronic Data) ~rn~ ~~ :::c "0 o POTWIWWTP Format: o~:-g co 0) () c: Comments: Receipt Temp ~«(J)1.2 ~ ::J U ;tJ fir °c o State: o LEVEL IV o L.-aJl c.: ~ e --cu c: ·c ~ co '-cu.-00 a c o Other: o NELAC ~~l~:i ~ ~ .... On Ice: y® :J ::J(J)--(J) ct -l-S zo.<CI5rO c-( w -0 Custody Seal '-~ >1 UJ CO On Bottle c:!> N C/) "'0 (/') 4 c On Cooler . N ~ CO ~N ..... H Intact C/) SAMPLE IDENTIFICATION Collection Collection MATRIX' ~ Signature G)N {Name, Location, Interval, etc.) Date Time Match 1 f .. ·v, .'/-)( Alor-l-~ £~+-Lt/u/l ~ Oqoo ~ 2No~tk lIJc,s+-...,llt/t'l.. ~o~o j .. V )( IX ~ 3 WeS+--14JH/'~ 1'2.00 t -V lX )( \QJ St)u t~ Innn 4 ~ 5 1<::::::1 ~ 6 ~ 7 ~(J~~o1n~ 8 I, ~ 0) 9 " 10 I~ Custody Relinquished b)' {Prift. DateJTime: /.Signature: ell. Received by (print): OatelTime: Signature: Go..,..,. I A. ·'.1 Ai!.I'" 4· H· ,1.. ,I'll"} ''''Au:::::.. I ' .... -Record Relinquished by (print): Date/Time: Signature: Received by (print): Datemme: Signature: MUST be Signed Kecelvea DY LaDoratory: [)atel J Ime: ~;u~~: G: s: s< Sample Dispo~ Return to Client: Lab Disposal: t{-}~-Ja. T~~O In certain circumstanc$, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report_ Visit our web site at WWW.energylab.com for additional information, downloadable fee schedule, forms. and links. EI'ERGY LABORATORIES www.energylab.com Alialytical ExcsJlsns:s SiIlCB 1952 Helena, MT 871-472 .. 0711 • Billings, MT 800-735 .. 4489 • Casper, WY 888 .. 235 .. 0515 ~illette, WY 866~686 .. 1175 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 August 09, 2012 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C 12060622 ANALYTICAL SUMMARY REPORT Project Name: Late Spring Vegetation 2012 Energy Laboratories, Inc. Casper WY received the following 3 samples for Denison Mines USA Corp on 6/14/2012 for analysis. Sample ID Client Sample ID Collect Date Receive Date Matrix Test C12060622-001 North East 06/11/12 13:00 06/14/12 Vegetation Digestion, Radiochemistry Lead 210 Radium 226 C12060622-002 North West 06/11/12 12:15 06/14/12 Vegetation Same As Above C12060622-003 South West 06/11/12 13:30 06/14/12 Vegetation Same As Above The results as reported relate only to the item(s) submitted for testing. The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. If you have any questions regarding these test results, please call. Report Approved By: Digitally signed by Steve Carlston Date: 2012.08.11 17:20:51 -06:00 Page 1 of 9 WWN.energylab.com Analytical ExCSIisnl:B SiI1Cil 1952 Helena, MT 877-472-0711 • Billings, MT 800-735 .. 4489 • Casper, WY 888-235-0515 Gillette, WY8GS-GS6-7ll5 • Ra id Cit , SD 888-672-1225 • College Station, IX 888-690-2218 CLIENT: Denison Mines USA Corp Project: Late Spring Vegetation 2012 Report Date: 08/09/12 Sample Delivery Group: C12060622 CASE NARRATIVE PB21 0 ANALYSIS USNRC Regulatory Guide 4.14 provides guidance on Minimum Detectable Concentrations (MDC) that should be achieved in samples for this radionuclide. The sample-specific MDC for this sample could not be achieved due to significant matrix interferences, restricting the volume of sample to be used in the analysis. Please consult with your local regulatory agency prior to using these results for compliance purposes. ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-cs -Energy Laboratories, Inc. -College Station, TX CERTI FICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Tests associated with analyst identified as ELI-CS were subcontracted to Energy Laboratories, 415 Graham Rd., College Station, TX, EPA Number TX01520. Page 2 of9 EI'.ERGY LABORATORIES www.energylab.com Analytical ExCliIISIICB SiIlCB '.952 Helena., MT B17~412-0711 • Billings, MT BOO-735-4489 -Casper, WV 888-235-0515 . '9lne.#e, Wy 886~6B6-7175 • Rapid City, S!} 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Late Spring Vegetation 2012 Analyte Method: E903.0 Sample 10: MB-34130 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: LCS-34130 Radium 226 Sample 10: C12060979-006AMS Radium 226 Sample 10: C12060979-006AMSO Radium 226 Sample 10: MB-34170 Radium 226 Radium 226 precision (±) Radium 226 MDC Sample 10: LCS-34170 Radium 226 Qualifiers: RL -Analyte reporting limit. Count Result Units 3 Method Blank 3 0.007 pCi/g-dry 0.005 pCi/g-dry 0.006 pCi/g-dry Laboratory Control Sample 0.3 pCi/g-dry Sample Matrix Spike 3.5 pCi/g-dry Sample Matrix Spike Duplicate 3.6 pCi/g-dry Method Blank 0.00044 pCi/g-dry 0.00021 pCi/g-dry 0.00022 pCi/g-dry Laboratory Control Sample 0.014 pCi/g-dry MDC -Minimum detectable concentration Report Date: 08/09/12 Work Order: C12060622 RL %REC Low Limit High Limit Run: TENNELEC-3_12071 OB Run: TENNELEC-3_12071 OB 109 70 130 Run: TENNELEC-3_12071 OB 109 70 130 Run: TENNELEC-3_12071 OB 111 70 130 Run: TENNELEC-3_12071 OB Run: TENNELEC-3_12071 OB 104 70 130 NO -Not detected at the reporting limit. RPO RPOLimit Qual 1 .1 Batch: RA226-6096 07117/12 01 :44 07/17/12 01 :44 07/17/1201 :44 07/17/1201 :44 19.6 07/17/1201 :44 07/17/1201 :44 Page 6 of9 EI\ERGY LABORATORIES www.energylab.com AIl8IyticaI ExcsllSiICB Sim;g '952 "..:. . Helena, MTB17-472-071 t • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 GiIf~!te, wY 866-,86-7115 • Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: Late Spring Vegetation 2012 Analyte Count Result Units Method: E909.0 Sample 10: MB-16690 Lead 210 Lead 210 precision (±) Lead 210 MDC Sample 10: LCS-16690 Lead 210 Sample 10: C12060622-001AMS Lead 210 Sample 10: C12060622-001AMSO Lead 210 Method: E909.0 Sample 10: MB-16690 Lead 210 Lead 210 precision (±) Lead 210 MDC Sample 10: LCS-16690 Lead 210 Sample 10: C12060622-001AMS Lead 210 Sample 10: C12060622-001 AMSO Lead 210 Qualifiers: RL -Analyte reporting limit. 3 3 MDC -Minimum detectable concentration Method Blank 3E-06 uCi/kg 2E-05 uCi/kg 3E-05 uCilkg Laboratory Control Sample 0.0023 uCi/kg Sample Matrix Spike 0.0013 uCilkg Sample Matrix Spike Duplicate 0.0014 uCi/kg Method Blank 6E-06 uCi/kg 6E-06 uCi/kg 1 E-05 uCilkg Laboratory Control Sample 0.0022 uCi/kg Sample Matrix Spike 0.0013 uCi/kg Sample Matrix Spike Duplicate 0.0013 uCi/kg Report Date: 08/09/12 Work Order: C 12060622 RL %REC Low Limit High Limit RPO RPOLimit -Qual Run: SUB-T46565 Run: SUB-T46565 98 70 130 Run: SUB-T46565 107 70 130 Run: SUB-T46565 113 70 130 Run: SUB-T46565 Run: SUB-T46565 93 70 130 Run: SUB-T46565 104 70 130 Run: SUB-T46565 107 70 130 NO -Not detected at the reporting limit. -5.7 3.3 Batch: T _16690 07/30/1222:16 U 07/30/12 23:04 07/31/1200:39 07/31/1201 :27 14.7 Batch: T _16690R 08/02/12 00:01 U 08/02/12 04:27 08/02/12 13:19 08/02/12 17:45 12 U -Not detected at minimum detectable concentration Page 7 of 9 www.energylab.com Analytical ExcsIIIllCB SIne, 1952 EI\ERGY LA130RATORI ES Helena, MT 877~472-0711 11 Billings, MT 800-135-4489 • Casper, WY 888-235-0515 ,(m'ette,WY 86& .. &86 .. 7175 • ~apid City,S[) 888-672-1225 • College Station, IX 888-690-2218 . ,',',..... ".' ". " . Standard Reporting Procedures Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as -dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Workorder Receipt Checklist Denison Mines USA Corp Login completed by: Corinne Wagner Reviewed by: BL2000\kschroeder Reviewed Date: 6/19/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) ContainerlT emp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 28.8"C No Ice Yes 0 Yes 0 C12060622 Date Received: 6/14/2012 Received by: th No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 No 0 Carrier Ground name: Not Present 0 Not Present 0 Not Present 0 No VOA vials submitted 0 Not Applicable 0 Page 8 of9 ""U Q) co CD <0 o -<0 EN:RGY aIJ" Chain of Custody and Analytical Request Record Page~of~ ~ --- -----~ -~ ----------- ---~ -- Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: D eo,,·, -' C>tA. "v\ I of\" ,,5 L~t(... .sf"'\~~ V~~'; t~.ti 0""-~Ol"" State: Ur Yes !S No 0 Report Mail Address: PO ~o)( gOq Contact Name: Phone/Fax: Email: Sampler: (Please Print) gl~tA~lI'\.~ VI ~YSU 6t>.,.-r;"... ~~\~t:r" 435 67£ ~a.~\ 6~c-\A. Pl-w\~ Invoice Address: Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: s.()..~~ 5A..~e- Special Report/Formats: ~&[b \1@U@ OO§@@~§lID .. Contact ELI prior to Shipped by: s: iA1$-L.., Cl Q) RUSH sample submittal ~o C/}..c:. ~ for charges and Cooter IO{s): , ~1D~OI Q) 0 « R scheduling -See Cl.~~ ._> 0 >.10 W t:, I nstruction Page Dow D EDD/EDT(Electronic Data) ~(/)~ m!i: 0s:= ~ C) J: "0 Receipt Temp o POTWIWWTP () c:: Comments: Format: U«~I.Q~ ~ U ~O. Yoc o .... CCI c: ~ « 0 o State: o LEVEL IV !... (U.s t= .i:: ~ I-ro ~ a..CtJ.Q 0 c:: -D Other: o NELAC ~Iro • ~ I-On Ice: y-U -~ ::::I <1>-= Q5 $: d d ~ 5 zo..«l~o W "'E Custody Seal ~ >1 W ro On Bottle ~~ en "0 en ~ ~ c:: On Cooler S H Intact en SAMPLE IDENTIFICATION Collection Collection MATRIX Signature (Name, Location, Interval, etc.) Date Time Match 1 6/1I/1~ ,-\I )( X No f'"" t-k £....,S + 1'300 i~ 2 AJOr-.... ~ We-5 ..... bIll /12 12.15 I-V )( X ~ 3 L..>~.t+ t/U/I(J.. I?' 'lO I-V X X cgy ~tl()-t~ nnn 4 ~ 5 F=' ~ 6 ~;louO/.lA?t 7 ~ ~ 8 I~ 0) 9 I~ 10 !r:J Custody Relinquished by (print): Date;ii~, 11!2 J, sOD Signature: al. Received by (print): Datemme: Signature: bc. .. r' ~ PA.I"",U-/ ~-'" .... Record Relinquished by (print): Datemme: I-Signature: Received by (print): DaterTime: Signature: MUST be Signed Kecelvea DY Laooratory: uateJI lme: /~~C;> ;gil~ lJeIJ.-{ Sample Disposal: Return to Client: Lab Disposal: ~.-, 4-I ~ .-:T -.". In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order 10 complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. ATTACHMENT G STACK SAMPLE LABORATORY RESULTS Prepared for: FIRST QUARTER RADIONtJCLIDE EMISSIONS TEST CONDUCTED AT DENISON MINES CORPORATION NORTH YELLO\V CAKE SCRUBBER YELLOW CAI(E DRYER BAGHO·USE BLANDING, UTAH Febrtulry 28-29, 2012 by: TETCO 391 East 620 South American Fork, UT 84003 Phone (801) 492-9106 Fax (801) 492-9107 fax Denison Mines Corporation 6425 S Hwy 91 Blanding, Utah 84511 April 3, 2012 CERTIFICATION OF REPORT INTEGRITY Technical Enlissions Testing COlnpany (TETCO) certifies that this report represents the truth as well as can be derived by the methods employed. Every effort was made to obtain accurate and representative data and to comply with procedures set forth in the Federal Register. Mike McNamara 111, J Revi ewer: I~~~/ IIAA~,dt.t",,- --~~~~---------------------- Date: ___ L{--L/_k-:....{ 1---.:' ,~z.,,---____ _ ii TABLE OF CONTENTS Introduction Test })urpose ......................................................................................................................... 1 Test Location and Type of Process ...................................................................................... 1 Test Dates ............................................................................................................................. 1 Pollutants Tested and Methods Applied .............................................................................. 1 Test Participants ................................................................ , .................................................. 2 Deviations frOll1 EPA Methods ........................................................................................... .2 Quality Assltrance ................................................................................................................ 2 Surl11nary of Results En1issio.11 ·Reslllts .................................................................................................................. 3 Process Data ...................................................................... , .................................................. 3 Description of Collected Samples ........................................................................................ 3 Discussion of Errors or Irregularities ................................................................................... 3 Percellt lsokinetics ............................................................................................................... 4 Source Operation Process Control Devices Operation .............................................................................. ; ...... 5 Process Representativeness .................................................................................................. 5 Sampling and Analysis Procedures Sanlpling POl11,ocation ....................................................................................................... 6 Sanlplirlg Point Location ...................................................................................................... 6 Salnpling Traitl Descriptioll ................................................................................................. 6 Sampling and Analytical Procedures ................................................................................... 7 Quality Assurance ................................................................................................................ 7 Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence III Table I II III IV V Figure LIST OF TABLES Measured Radionuclide Emissions ..................................................................................... .3 Percent lsokinetics ............................................................................................................... 4 Sampling Point Location ...................................................................................................... 6 COlnpiete Results, North Yellow Cake Scrubber .............................................. Appendix A Complete Results, Yellow Cake Dryer 8aghouse ............................................. Appendix A LIST OF FIGURES 1 Facility Schematic Representation North Yellow Cake Scrubber ..................... Appendix D 2 Facility Schematic Representation Yellow Cake Dryer Baghouse .................... Appendix D 3 Schelnatic of Method 51114 Sampling Train ..................................................... Appendix E iv INTRODUCTION Test Pur[!ose This test project was conducted to determine the total radiol1uclide emissions frOln the North Yellow Cake Scrubber and the Yellow Cake Dryer Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dsct). These tests were for U-Nat only. Test Location and Type of Process Denison Mines (USA) Corporation is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scrubbers. Both dryer enclosures discharge into the Yellc)\,v Cake Dryer Baghouse. 'fhe packaging enclosure also discharges into the Yellow Cake Dryer Baghouse. The North Yellow Cake (NYC) dryer was the only operating dryer at the time of the test. The South Yellow Cake dryer is currently not operational. The Grizzly Baghouse serves as the main dust control device for the raw ore unloading and conveying to the processing building. Stack schematics are shown as Figures 1 and 2 in Appendix D. Test Dates One test run was completed on the NYC Scrubber February 28, 2012 and one run on February 29th . One run was completed on the Yellow Cake Dryer Baghouse February 29. 2012. Pollutants Tested and Metbods Applied The tests were a determination of radionuclide emissions in accordance with EPA Method 5/114. Test run filters and front wash residues were sent to Test America located in Richland, Washington for radionuclide analysis. Test Participants Test Facility State Agency TETCO Garren P alnler None Doug Olsen Jeff Graton Deviations From EPA Methods None QuaHtv Assurance lVlike I\1cNamara Testing procedures and sample recovery techniques were according to those outlined in the Federal Register and the Quality Assurance Handbook/hr Air Pollution jV1easUremenll~)istems. 2 SUNIMARY OF RESULTS Emission Results Table I presents the fIndings of the test in Curies per dry standard cubic foot. Tables IV,-V I in Appendix A have lTIore detailed information. Table L Measured R~ldionudide Emissions North Yellow Cake Scrubber Yellow Cake Dryer Baghouse Run # pCildscf pCi/hl' pCi/dscf pCi/hr 274.9 2.019E +07 17.9 2.251E+06 2 358.5 2.712E+07 AVE 316.7 2.36SE+07 Process Data The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow, pressure drop readings (~p) were recorded and are found in Appendix D. The Dryer Baghouse pressure drop readings (~p) were recorded and are found on the test run sheets. Production data will be submitted by Denison Iv1ines. Description of Collected Sanlples The test filters for the North Yellow Cake Scrubber were heavily covered with a white or pinkish white colored patiiculate. The front washes were clear in appearance. The test filters for the YelJovv Cake Dryer Baghouse were lightly colored with a tan colored particulate. The front wash was clear in appearance. Discussion of Errors or Irregularities None 3 Percent lsokinetic Sampling Each test run was isokinetic within the ± 1 O°lc) of 100'Y<) criterion specified in the Federal Register. lsokinetic values for each test run are presented in Table n. Table H. Perc(~nt IsoB{inetic Sampling North Yello\v Cake Yellow Cake Dryer Run # Scrubber Baghouse 1 106 96 2 97 4 SOURCE OPERATION Process Control Devices Operation All process control devices were operated normally. Recorded scrubber water f1ow, pressure and baghouse .6p readings were recorded and are found on the test run sheets or in Appendix D. Process Representativeness The facility was operated normally. Production data was retained by Denison Mines. 5 SAMPLING AND ANALYSIS PROCEDURES SamplingRQ[t Location The inside diameter of the NOlih Yellow Cake Scrubber stack is 18.0 inches. The two, f-our-inch diameter smnple pOli are located 6.3 diameters (9.5 feet) downstream from the last disturbance and 6.3 diameters (9.5 feet) upstream from the next disturbance. Figure 1 in Appendix 0 is a schenlatic of the stacie The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch diameter sample ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 diameters (57 inches) upstream from the next disturbance.' The sample port locations are depicted in Figure 2 in Appendix D. Sanipling Point Location. Table HI shovvs the distance of each san1pling point from the inside wall according to EPA Method 1. Each point is ll1arked and identifIed with a wrapping of glass tape and numbered. These points are determined by 111easuring the distance from the inside wall. Table Ill. Sanlpling Point Location Distance (inches) from Inside Wall Sample Point NYC Scrubber Dlyer Baghouse 0.58 0.70 2 1.89 2.34 ') 3.49 4.74 .J 4 5.81 ] 1.26 5 12.19 13.66 6 14.51 15.30 7 16.1 ] 8 17.42 SanapUng Train Descaoiption To determine the actual emission rates for this stack, 40 CFR 60, Appendix A, ivlethods 1-5/1 ] 4 were followed. 6 All sampling trains were made of inert materials, (Te-tlon, stainless steel and glass) to prevent interference of the smnpled gas and particulate. The stack analyzers used to conduct Methods 1- 5/] 14 are constructed to meet the specifications outlined in the CFR. The temperature sensors are K-type thennocouples. Heater, vacuum and pitot line connections have been designed to be interchangeable with all units used by the tester. A 316 stainiess steel probe liner was llsed for the tests. Figure 4 in Appendix E is a sketch of the I\1ethods 51114 sampling train. Sample boxes were prepared for testing by following the prescribed procedures oUllined in Methods 5/114. Sampling and Analvtical Procedures All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 5/114. Quality Assurance All equipment setup, sampling procedures, sample recovery and equipll1ent calibrations were carried out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbookfor A ir Pollution lvieasurement S:vstems. 7 APPENDIX A: COlnplete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence 8 APPENDIX A Table IV Complet.e Results, NOlih Yellow Cake Scrubber Table V Complete Results, Yellow Cake Dryer Baghouse Nomenclature Sample Equations A NYC Se,ubb., TABLE IV CO MPLETE RESULTS DENISON MINES CORPORATION, BLANDING, UTAH NORTH YELLOWCAKE SCRUBBER EXHAUST Symbol Description Dimensions Run #1 Run #2 Date 2128/2012 2/2912012 Filter # 5866 5868 Begin Time Test Began 7:53 7:37 End Time Test Ended 16:04 15:45 Pbm Meter Barometric Pressure In. Hg. Abs 24.20 24.50 ~H Orifice Pressure Drop In H20 1.350 1.148 Y Meter Calibration Y Factor dimensionless 1.004 1.004 Vm Volume Gas Sampled--Meter Conditions cf 359.519 335.279 Tm Avg Meter Temperature of 94.0 96.3 --.J~P Sq Root Velocity Head Root In. H2O 0.2628 0.2615 W1wc Weight Water Collected Grams 706.6 502.6 T t Duration of Test Minutes 480 480 Cp Pitot Tube Coefficient Dimensionless 0.84 0.84 Dn Nozzle Diameter Inches 0.3810 0.3810 C O2 Volume % Carbon Dioxide Percent 2.90 2.80 O2 Volume % Oxygen Percent 16.30 16.30 N 2 &CO Volume % Nitrogen and Carbon Monoxide Percent 80.80 80.90 Vmstd Volume Gas Sampled (Standard) dscf 279.391 262.521 Vw Volume Water Vapor scf 33.316 23.698 Bws (measured) Fraction H20 in Stack Gas (Measured) Fraction 0.107 0.083 Bws (saturated) Fraction H20 in Stack Gas (Saturated) Fraction 0.120 0.095 B ws Fraction H20 in Stack Gas * Fraction 0.107 0.083 Xd Fraction of Dry Gas Fraction 0.893 0.917 Md Molecular Wt. Dry Gas lbllbmol 29.12 29.10 Ms Molecular Wt. Stack Gas lb/lbmol 27.93 28.18 %1 Percent Isokinetic Percent 106.1 96.8 AVG Ts Avg Stack Temperature of 113.9 106.3 110.1 As Stack Cross Sectional Area Sq. Ft. 1.767 1.767 P G Stack Static Pressure In H20 -0.055 -0.055 Pb p Sample Port Barometric Pressure In. Hg. Abs 24.13 24.43 P s Stack Pressure In Hg. Abs 24.126 24.426 Qs Stack Gas Volumetric Flow Rate (Std) dscfm 1.22E+03 1.26E+03 1.24E+03 Qa Stack Gas Volumetric Flow Rate (Actual) cfm 1.85E+03 1.81E+03 1.83E+03 Vs Velocity of Stack Gas fpm 1.04E+03 1.02E+03 1.03E+03 Curies Radionuclides per sample pCi 76800.0 94110.0 Crad Concentration of Radionuclides pCildscf 274.884 358.486 316.685 ERrad Emission Rate of Radionuclides pCiIhr 2.019E+07 2.712E+07 2.365E+07 * lfthe measured moisture content is greater than the saturated moisture level (supersaturated), the saturated moisture value will be used in all calculations (40 CFR 60, Method 4, Section 12.1.7). Symbol Date Filter # Begin End Pbm 6.H Y Vm Till -Y6.P \VtW(; Tt ep Dn CO2 O2 N2 &CO Vrnstd Vw Bws Xci Md Ms %1 Ts As Po Pbp Ps 05 Qa Vs Curies Crad ERrad TABLE V COMPLETE RESULTS, PM DENISON MINES CORPORATION YELLOW CAKE DRYER BAGHOUSE Description Dimensions Run #1 Dale 2/29i2 0 12 5865 Time Test 8egan 8:08 Time Test Ended 10: 13 Mete.r Baromcrric Pressure: Ill. fig Abs 24.50 Orific.e Pressure Drop In. Hi () 1.273 Meter Calibration Y Factor dimensionless 1.004 VolulJle Gas Sampkd--l'v1eter Conditions .:1' 90.610 Avg Meier Temperature of 90.6 Sq Root Velocity Head Rout In H2O 0.4968 Weight Wakr Collected Grams 9.5 Duration of Test Minules 120 Pitot Tube Coenicicilt DllllCIlSIOllleSS 0.84 Nozzle Diamder Inches 0.2765 Volume 0,';, Carboll Dioxide l''<:recnt 0.00 Volume % Oxygen Percent 20.90 Volume %, NitTogen and Carbon Monoxide Percent 79.10 Volume Gas Sampled (Standard) dsef 71 .708 Volume Water Vapor scf 0.448 Fraction I-Ill) ill Stack Gas fraction 0.006 Fraction of' Dry Gas Fraction 0.994 Molecular WI. Dry Gas Ib !Jb 1110 I 28.84 MoktularWt. Stack Gas Ibilblllol 28.77 Percent Isokindic Percellt 95.6 Avg Stack Temperature "F 71.9 Stack Cross Sectional Area Sq. FL 1.396 Stack Sintic Prcssure Ill. H2O -0.2 J Sample Port Barometric Pressure Ill. Hg. Abs 24.43 Stack Pressnre 111. Hg. Abs 24.415 Slack Gas Volumctric Flow Rate (Std) dsclin 2.09E+03 Stack Gas Volumetric Flow Rale (Actual) cfl11 2.60E+03 Velocity or Stack Gas rpm 1.86E+03 Radionuciides per sample pei 1285.0 Concentration of Ratliolluclides pCi/dscf 17.9198 Emission Rate of Radiolllldides pCi/hr 2.251 E+06 Dryer Ba9house M5 Nomenclature %1 = percent isokinetic, percent A = stack cross-sectional area (ftJ) s ASflP = see --,JL\P Btu = unit heat value (British thermal unit) Bws = II'action of water in stack gas Cn = concentration of particulate matter, back half (gr/dscf,lb/dscf, etc.) Cr = concentration of particulate matter, front half (gr/clscf~lb/clscf~ etc.) Cmetal = concentration of metals (ppm, ~Lglftj, etc.) atomic symbol replaces "metal" CO2 = percent carbon dioxide in the stack gas Cp = pitot tube coefficient (0.84) C -sJ)ecies symbol rel)laces x. x (nvg)- C.y (corr) = actual gas concentration corrected to required percent O2 L\H = orifice pressure drop (inches H20) L~H@ = orifice pressure (inches H20) SP = stack flow pressure differential (inches H20) Os = diameter of the stack (feet) On = nozzle diameter (inches) EA = percent excess air ERB = emission rate of back half particulate (lb/hr) ERr = emission rate of front half particulate (Ib/hr) ERl11l11Blu = emission rate per mmBtu or tOil of fuel etc. ERx = emission rate of compound which replaces x k-fact = multiplier of test point AP to determine test point AH L = length of rectangular stack (inches) mBtu = thousand Btu Md = molecular v.leight of stack gas, dry basis (I b/Jb-mol) M.: = mass of particulate on filter (mg) MFP = mass of paltlculate matter on filter and probe (mg) mmBtu = million Btu Mp = mass of patticulate matter in probe (mg) Ms = molecular weight of stack gas, wet basis (g/gmol) N1 = percent nitrogen in the stack gas O2 = percent oxygen in the stack gas .y!).p = average of the square roots of.6.P (may also be referred to as AS!)'P) Pbm = absolute barometric pressure at the dry gas meter (inches Hg) Pbp = absolute barometric pressure at the sample location (inches Hg) Pc; = stack static pressure (inches H20) Ps = absolute stack pressure (inches Hg) Pstd = absolute pressure at standard conditions (29.92 inches Hg.) e = time of test (minutes) Qa = stack gas volumetric flow rate (actIn) Os = stack gas volumetric flow rate (dscfm) Ow = wet stack gas std. volumetric flow (fr)/min, wscfm) Tm = meter temperature tF) Ts = stack temperature (OF) Tstd = absolute temperature at standard conditions (52SoR) Tt = see e Urn = mean molecular speed (cm/s) Vm = salnple volume (tt3) at meter conditions M5 Nomenclature Vmstd = volume standard (dsef), sample volume adjusted to 6SoF and 29.92 inches Hg. V s = velocity of stack gas (fpm) Vwc = volume water vapor (set) at 6Sor and 29.92 inches Hg. W = \\licIth of rectangular staek (inches) Wtwc = weight of the condensed water collected (grams) Xd = fraction of dry gas Y = meter calibration V-factor (dimensionless) Method 5 %1 = Vmstd" (Ts + 460)" 1039! (8" Yo." Ps " Xci" Dn~) As = Ds:! / 4" n Bws = Vw / (Vmstd +Vw) eB == MB IJ 0.01543 ! Vmstd Cf == Mrp" 0.01543 / Vmstd ex (corr) = ex (avg) .. (20.9 -desired %02) ! (20.9 -actual %02) Deq = 2 .. L .. W / (L + W) EA = (%02 -0.5 %CO) / [0 .264 %N2 -(%02 -0.5 %CO)] ERg = Cn ., Qs co 0.00857 ERF = Cr " Os e 0.00857 ERI1111lBtu = ERx / (mmBtli / hr) K-fact= 846.72 .. Dn4" ~H((i} 0 Cp 2 eX}" MJ .. Ps" (Tm + 460) / [Ms co (Ts + 460)" (Pbrn + L.\H ! 13 .6)1 Md = CO2 '' 0.44 + O2 " 0.32 + N2 .. 0.28 Ms = (Mu .. Xd) + (1 8 .. Bws) Ps = Pbp + (PC) ! 13.6) Qa = Vs" As Qs = Qa" Xci .. Ps .. Tstd ! [(Ts + 460) ill pstdJ Qw = Qs / Xd Vmstd = Vm" Y" TstJ " (Pbm + ~H 11 3.6) I [Pstd" (Till + 460)J V:; = 85.49 .. 60 .. Cp .. ~~P G -V [(Ts + 460) / (P~ .. Ms)] Vwc = Wtwc @ 0.04715 Xd = 1 -Bw~ APPENDIX B N0l1h Yellow Cake Scrubber Preliminary Velocity Traverse and Sampling Point Location Data Particulate Field Data YeHow Cake Dryer Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Pmiicuiate Field Data B North Yellow Cake Dryer Scrubber Prelim 8 pts blank Facility Denison Mi nes Stack rdenti ficati on North Yellow Cake Scrubber Date - r Barometric Pressure Pblrl 1" 'i ·S;,) in Hg Pbp L'-1,<t5 in j-Io '" N 0 Static Pressure (Pd --O· J ~~jn /-1;:0 B Esti mated Moisture (BwJ i.!5.. . .J % Samp le Height from Grollnd 7-0 feet A Comments: Stack Dia 18 Reference: 0 Ports nre 9.5' Upstream from next disturbance Ports arc· 9.5' Downstream !rom last disturbance Traverse Percent Distance From: Ports Point Diameter ID Reference A B C D E F I 3.2 0.58 0.58 2 10.5 1.89 1.89 . 6S'-II (- " 19.4 3.49 3.49 .) 4 32.3 5.81 5.8 1 . ().) --!IV .5 67.7 12.19 12.19 6 80.6 14.5 1 14.5 1 -j}(" ~!(" 7 89.5 16.1 ] 16.1 1 8 96.8 17.42 17.42 .O(P;;;~1- -- Averages: 1's L Flow ---- flP L Flowl ~p . KEY=> q.. .. ~ s 5g-~ &/ s:8-t :}- _ "\ Ld TLTCO Filte~ Sample [ill'; Ii held l)<,la Sheel l'I<lIIl. Iknisu(l i'dines I)alc 2--tV llv 1.\'CallDIl North YJ<Sllo\\cakl' Dn'cr Scruhher ()pn,II('r ~ , I n.iH~rSe Tlmc f)(jivl .\p \H (!pH,C)) V~H.:tlUIl\ Tcmpcratures ,'" [)(j!\1 1 <:'~II',II..'.'~_ POInt t CI()c\: Min (0) dt..': 1)1;1\\), "\)~'~I'~~~;'! /\ (; ll~;;;' ,u;l[,.:, Slack I, l',J Probc hob-:,UlIt I:ilter I :fllucl1t Ow III =R lLS2 a ~af.5?(;o ·O4l,'"' .~ { .S' \ I~ II V . 'Z...<tt 1,{ti ?{it-,'1 Is-'6 5"2 15 JA?o~1'VI ·bG'0 ·~tV ·tiD "'l/ 1111/ 1, '\) 'L~I) .'1~ 1, ~q r;;f:) ~ ~ 30 ( O{!.?·I&q "o5:F [·01 I-D\ ~ t {\ 1,,--l~ ZG?"Lr -z...~'{ l.{{ L()Co ~ 2 45 I J D ~D./"'t'1 ;0\;(:> /.(L '-10 !1/ no 1., ~\ 7 t{tJ -z, 1. $'{ 1..\, 1-, t1), 3 60 i fO~V ·l~~ -~~ f .1-, {.t2 ~ , I t-O. ~q 1.[;("" t~b 4Y ~v ~~ 3 75 :1 bi.{! ·t5"'~ . D(.f' 1/J.1.-5 !·t~ ? lt~ rz-. &0 1,V{'{-1.,&~ .~~ ~ tD'f 4 90 loSt.. "$)1...-.O~7 I-'i"'i \-,-!vJ '> d~ Z5co. z,S-q '7.c'& 1rtj 10 4 105 II nW . <i;'~i~ ~o~o I'~r (.~~ ~ It) 1--5"_'1 fl/J 'Z~, (Lr ~+-[Dr 5 120 1/6111· -~~1 '·o~~ J • fit.{ (·l1!J '-I \\~ t ~t.-'2. tfi. ~ U~ q~ lOS 5 135 IJ1)~,~W .. DcjQ j .1-L! I·:}Y e:;. t tvl 1.-lv) 1. (I & 'Lf"'f 1'; LQ~ ~ 150 Hb[.'1'lA • DC] (' 1-1'1 ( .1-~ ~ E' 2.vt( 1 r~s 1);0 l()-O)j ..lid 165 ·TII~ .. ·~1\ ,~~ {-¥t;; (·e>-! S H~ -1J.~~ I t:. ;,~ '1..-Slc ~~ Pl~ I( 0 7 I 180 1I'L5S/~'i -oo,D ! l/+\o ,.1{0 , U H\., LSV\ 1 ,V~, 1,$--)-5j "1'1 !I( 7 i 195 i I '1 i ! VJ f -ct1C I· fr<; [(ere LO \ \c:? ji)"1 1, (o-t rJ.t;-\ ,,\ c,<; itO r--' ,-??;--CjC( '(o'f 8 /210 1}&~·5z:) ·o0() 1·1~ r·~~ ~ \t~ 2(t? "t 1,!j -t 1 ~t:" _ .. ,I 8 225 {l{gr.>} v 'o$f)' i.ltv !.(,,~ or:y tf(p h Io~ 'l19 ) 1~A ')') ")'3 10lO 240 II rsO.l<;() ..... ----- -- I -' -_ .. _-----'--'----_.- ---i ~ ----, --.l I ---, ... =11-~11 81 I -iR~IRR '1'0(:11 I K~. ~~> i\\Cn'!~I: I I i DGM before Leak Cheek I VaetHg) Rate (fe/min) DGM After Leak Check Vac ("Hg) I , \ ~ O. l C( ') I IL\ D-o'O(o !/¥{) . ¥ 0 r ~ ! fo.So( f~ i I i I I I i ---.. -~-I I I I I I'ag~ or ~. I~ull i; i /'~\ B (,-J N A SI;lCl-Dlametcr I~" Purt RclCrCIKC \I (I" ll\lrt, af(; 9.5' lJp~(rc<l111 1'rul11 nexl dlsturball!;c 1'",(:-,;ItC' 9.5' 1)"'\i'l,trc',ul11""111 Llstdl'(ttrballc(,; !\~'lIll1\:d tviulslUl'C 4·13"" I)rp!lc .1.1 -!t> ('p 0.84 ~~ol.llc Calibratloll :~" 1ft ",,~,:r( oW! (la!'l3ag~ l.'u 11 SO il' (g '(·1',1«(01' t· 00'-/ \H® /_ (, (ft, III Il,U Lo,::ak CIH:{.:k Ibl'lllllctI'lC I'ICS:<urC, I'!l", 2-c.{. ~O I'b, Zc.(. ( 3 I).. ' 0 (j'J ..... L'L~ "'"",, D·Do' \;(C '" II~ 2....3. PlInt R.llc _ ~. 0 li'lh()~ o .2i Wakl' '. 'ullcclcd 1Illig 111 Ilg III II ,~() \'.118 \ lillC :->'.lInpkl\ l1111l I~l:\ IL'\\ k ({ j"" {I:I'III Rate (felr!!}.r:!J _ D< t ori /' <v,b p\) Field Data Sheet Plant: ---4--~ Date / ... ~& -r 0.6\.'0 ~TETCO 4-~r~~__ Sample Box ________________ _ -'---'---_.-_._--" -------.~ .. -,.---.-.---.. - Location North'(el)lowcake Dryer Scrubber Operator: b \ L\P ,:\H un ;-1;(;1 II Vacuum I Temperatures ,.--1" DGiVf T~l11p (T",) Probe Filter DGM Traverse II TIme POlllt Clock I Min (8) '~'" Ii.) II Stack (TJ Efnuent II Out I In IIi"; DeSIred I Actual '[lill:U) 1 II t2i~1 240 IllkO.<f;O [ II.o5'oll·Q"'t I·~{" II V Il u<: 1'7;0-' 'Z~f1'Z-,;14~_J~11 <10 1 II I 255 II I Ci 0 . ~t.!'{ II· D ~O II . '1 YI~~+-Ilm mv II ;, i~~ ~~{ l'LvtJ Ilq'-pj-C( (; II '§-k'i Cz & 2!l I 270 II l c1lt;· C(DVjI ~ O}Q II t'i'¥ I ~q::r II '{/ II J rt1] ~l!~n.~_lihlJ t{(; II ~g I '1 V 2 II I 285 II -Z~.~3-) II .. ec.t~ II .'O'{ r-·-~q II"")... tiC, It",{ 12.(...~ I 2."-( J ~ e II ~8 I 1-:( 3 II I 300 112\~.r{~O 11 ·\')~\Qj1 ~~'\I '~f1'li~I' Hlo I1.t('ltIU(11'){1 U~ lIC6yl ,5' 3 II I 315 11~~1.{pWJL·\)st>lL,-_~11=~"lj1 /tV 11\('±-ri.2LJ1.i~1LJZ_d1~1 vY I t) (P --W 330 ~ 345 5 I 360 ~ 375 6 II I 390 " tG),J 3 i JrnQ]~Ltf5ILL[JLu~ 1 'it; \ r-i-;O I iJ../61 {;-_;, II ~-'~ I frY; 6 1\ I 405 II 'l~rq[i~~II·D14\~~~I\·~5 JI q /I ll~r 11~~~iJ1.:)?I~t(D' ~0-11 O!S"'I fO\( 7 II I ~. 0\0·2;\ I :~lJS-I[gJL?W~ 1;;\ 1 Y19-61 I 435 1~~5'_1 __ '.Q. D ,"'Sf .~~Jl[ll[t "'t;l.]t; 1)·~lt (L'7J~ ;:;..15 I 7 8 8 Total f\v~r~1ge 450 II ~lOj __ ~1-l{ II . 0 ~1JU .~ ~Jr-..{JSJ~ II \ lYm .. _ L~75ri\!Pl t~1 ~ V II q~' It 01-, 465 n1,4r:\~Dvll -61111 { ·ql)'Tl .. ~s1 L.\ ' II \.l ~ -11 ~~1/\ 1,.-+\ 11-~,HY \ ~1/ 1101<6 I ! ,),'1 II itl;O Y 480 11i;t)t-t1~~ II II -~ II \ Ll:t . \'3 C.f! II J~~~~3 81 IHI I .II '7771, )!cr /',,_ Co· ~~~ "\ 0{~ S~ ---~\prJ.\P 'I' .1,;\P 't ~ \ .... ~5° \\7'~ -~ ------ DGM before Leak Check Vac ("Hg) Rate (fe/min) ----------I ---- l _V') t DGM After Leak Check _ ~'~{)f~ ~,:u I -------------- &olt) /- C1L{·O Vac ("Hg) Page Z. 01:..._2. Run Ii ----... 1. I N "0 A Stack Diameter I S" Port Reference 0.0" Ports are 9.5' Upstream from next disturbance Ports are 9.5' Downstrenm from last disturbance Assumed Moisture Probe ill 4-13 % Cp 0.84 ! N~7~~,-\alib~atio~(. • ,f5~ A'g D, ~. ;,,,',,' -, _ \\{ -? . ~~! (las Bag n'- Console t? '{-Factor ~{ i\H@ ~ V in l-[~O Barometric Pressures ~~,:,_-l~~~~-~----:~ ~~: Pi ,1 ___ :':~~:~Q_~l_ in H~O Leak Check pr~ fr"lllin fI vae .n Hg --+-'-\- {'Hot Rate In H,O _...J/'--__ Post O,OD ::) ~ i2SL-\'~Lf \1'-\ -""' ' Wattr Colb;t~d tO~ . 0 T:me Sampled I f g U g . RCVIC\\ Rate (fe/min) K K r\ mIn \ 1 kr'-\ \ '~?Yr'TI '(]"T", 1'lCld Data Sla:Cl !'Ialli' Iknis()~l rVlj~lCS Date t-n.:\ \ i'1 d' \ \ . I fa\ {~l~(.· '1'1111(; I)(jtv! ,\p \H HfIH.()} POltll Clock Min(U) 1\'1 ,iii } f .{ ~. I)csircd i\ctu~li ~ 1-:;1 0 -z,S'z..·YOD • f)S-O .~~", .. ~? 1 15 -;~I.ov5 · 0;5"1 j0!t ,"l~ 2 30 ~i-\. \,f1,'V "Clf" I ~vy' . irY .. ~ 2 45 ;t(,Lt?~V ·t;.i?' ~¥li ·~I 3 60 ';fC-j· vt t~ ,O(PD I ~ q-:r-. '1-=+ 3 75 1,C1C,. (p&{p fI .~~ .~V 4 90 1r;t:o .~'1f{ .' i, .X'(( , C(~ 4 105 'f !~.t}'1 ,. c){;Oi .'11-.q1- 5 120 42r. ~ 'Z:j.-:0 I ·l~ ['1 S- 5 135 L{')? ~~v: .0'15 f .1"1 f ,-ty 6 , 150 __ ~~q. rt-s."-J o~t) /·',V \ .)'1/ 6 165 ~~O .1,~,-\ I ·O~~' l'i O I ·~I D =H 180 1~1-1 ·0{~ 'of~ 1'<-/'0--/.'1 & 195 i \..{~-;. t{ [0-D":'&2iftl( ( 'e;'O ,-CO 210 l-i'1S. bJ~ · D4s g" t -v(L \ -'i"t. 8 225 !L)b!O·~I~ 'bk("' ( I"rl I \v( c. IL'j "\-' 240 e:; f S<. ~~ lI\ --)--- -------.-J ---ll I II IRI I J 'j ulal l &~.l{~~1 1\\ ('ragl' Leak Check Vac("H ---~- V' J IT H 'OA h iler (iJ1 £" Sumple [hI' f'T I,OC,lti()1l Norlirl'¥" L'llo\\'cakc 1)1'\ l~r Scrllblx:r (.lpc:ralol \f7\, ' \',h:IHJtll TCl1lpc:r;lillrc~;, 'I , D(i,,! f'clIljl ! I,,,i 111111:.1' Stac:k 1'1',1 I'robe ('/i.,IIl..: (hI! I'liiel U tlUL:1l1 UI.II 111 "//' f 0'1, t--1-"0 7,,:f-D t i{1O t.(-& tL'j '"+-1 'V l\?~ /I~10 -"LS'"'O "L<.{; t.{(p "t ~ <7b 1...-'O~ 1.,.uv 1, ~O z.~U 5'1/ t--:r 0) ,'" .v ~ loq 1,}O U~S--2.'(.,('1 ~:) Sf1/ '13 "v loS-1.-c;c 1 &<1 1j·.("7 <;'1 ¥~-'4'1 ~ 10) wI 2.&~ Zc.{ "). 5T' ~(p ~,,(j 'i'/ 1010 t.~j ~~l.-\ ~~~ ~fo !f;T' qc, 1/ Jt:.~ 1.,,&0 ZVS-Z.<..f,D ¢Z-~V q..-q. 'I, i {)~t ZS¥? 1,&& -z,'-1h -Sc., a;D '1'1 Ll1 , l of./ '~S'1 ~l{r -z,.t.{ t (~ Ctl lou ~I l o(P t10 zlPs-LSl-r C't1 C11, /O{ ~ ttk ~5) Thtt 7~ "'1 fp~ ~-C; 16ft; c;-I b.0. rJ_,UV /J Jtfi lU() S'y t1)"-tD${ c;-. t b -1" 70 f) 7. (,f Z~~ ~I..f 4(0 l()X' i G iOto l..\Q Q 1 {o v ~y.7./ ~\..-'1lo l o~ 1 (0 f D ~ 'LCp1, 7 {pC; 1J. ( ~\O qS-tOS' I FF L=t= Et= \LJ I -r -RI I _ II I Vac("H I)" I'al!,c t.lt' Z~ RUIl :: ~' i /--'\ N 8 -~) A Slar~ [)"lillder I X" I'uri Rl!krcJ1ce (10" Purt» are 9,5' l!p~II'caJll i'rum Ilcxt dlSillibal1Cc l'OIb ;11\: 9,5' 1 )()\\,Il~ln:alll i"r(JnJ la<.l ,k;turbClIlCl' i\~,'lIIlH:d IV!l)I~(1I4 l 4-1 3 "'0 Probe.: "'1 \7 ('p ~ Nou.lj: \jalilll:li\\\\\ f "2. .. ! q C. f . /)'1h .)~, . ~~'l • ')!,J ------- i\\g I)" .)~ \ 11)(;h,~o (Ja~ 13<1i!. U r:.. :> ~ "f \.. ~ l'clll~oll!~ )'-la\:1\)1 l· \it'l'1 ~ \H@ l'''i~9 III ti:U !~,an)lnelrl(' I>rcsstln.!::. I'bo;, '2. '(.S't> 11l11~ , V- I'lll' 2.1 -<) In llg, 1 C;1,('IIl'd, \;h,. I r I II ~~ 1)11,)( IbH' II,II:(J 1'" ,-o. O$"S" Iii liP I~!:,: ()·OC>~ ?..3 0 .0 ·1.4 -----...f- l'..\!~~ -..... \\';11<.:1 I, ',oIkl'lc,I ______ , Illllt,' ~<J1l1pIClI 1111 11 I~ -: \ Il'\\ ~ ({-I", }, liT,,, Rate (ft3/min) b ~blj& l'leld 1)~lt~1 Sheet l'lunl I )ellison ivlillc:-; , l i':TCO Idlci ~~,q SUlllPic Ilo.'I. 1.(lCallol1 Nmlh \'dIO\\cn!--c Dryer Scrllhb~~I' I)ak ________________ _ ( )pl'r~ll\lI" _______________ _ TinlC I r~;\ l"r:iC Ii __,.----------jl I)GM .\P ,\H 1m " .. 0; Temperatures ,'1 IX,,,;{ '\ e1l1!, ('1',,, J I\)llll Clock ,,', [)csJr(~d '\clllal Probe P",b"0", Fiilcr UlIucnt (Jul In i N l'il!'.'.~(lIVI,"I1 .. ;V 8 i~) ~T../ A 2 270 I'orl.' :11\' 9.5' llp~lrcalll 1'10111 no:\ JI~tlllhallc\~ l~Slack. DI<lI111'lCr IS" I'oil l,cIC!'CIlCc no" 2 285 Pori, ~lre. __ J..~.~· !)"I'n,trewll frolll laq disturbance' 3 300 3 315 4 330 4 345 5 360 5 ~37~5~~~~~~~~~~~~~~~~~~~ 6 390 6 1~40~5~~~~T+i~~~~~~~~~~1~~~~~~M~~~~"~~1 7 420 7 8 8 It;:'t> 435 ~ \; if j-liD-450 ~~ 1 _LLL 465 ~-q4 .~ 480 Vl./ -----11-----1---11 I ~~ ... \-{~q I~I I~f---II---·-.I I · ----l-.----+-... ------l!---..... -+-- I ,'lid !\\~r;'.Igc , . .~. _ ... ~I IWII-------+-----1 ,- ! (//1-£ I S; ~'.9 .3~~~7 \. .~ -z..r/j~ ..,./ ~/':? .v·\ \ \ ~ 1,1j\) ~io:rz,o ~l{D \ t' \ .V~~~ \ ch'~7 . ~ _. ( -_ ... .. _ ...... _ .... ~. .. DGM before Leak Check Vac ("H9)~ Rate (ft3/min) I DGM After Leak Check I I u l0) /' 01~·) Vac ("Hg) I I I /\~:'(lll1ll'd I\hJlSlUlC 4-13 "" I'rohe Z1:ltz I...'p 0.84 N~)}tra'il:~~ ~_ ,'3<6-( . "$ ¥ ) ;\vg I)" • 7'~ IIH:hc~ (;<t, Bag I-i£-5 CUI"uk {p )'·I:w,:(ol I -oo~ ,\H@J ,lea ((:1 III II:,() i3lll{ll1lctnc I'res~urc, Ph,,, '2-4, S'D 1111 k --3. -Phi' ? '-f. L( 111 fIg 1'" -o'05S 11\!1.:(l I "il" 'Ii," k I'lc I'(lsl Ii' 11111: ---- h!111 i\:Ift.' '------ 111[1,0_-""", __ O-OD) ~ o~D 0· 'L'Y f Wnlcl'CollcCl,:d 50Z'lP n III1K~ ~;lInpkd A Lf£'0 ~lIn Rate (fe/min) l\cllCil ~ I-.. u I", I( {/ I,,, t·~ \ (g< ~ Yellow Cake Dryer Baghouse Preli m 6 pts bl ank Facility Denison Mines Stack Id entification North Yellow Cake Dryer Baghollse Date - r Barometri(' Pressure B Pbll1 'Z-c{, .. .sa ttl Hg Php Gt/f, <0 in Hg -0 N Static Pressure (£leD CJ • vL in H2O A Estimated Moisture (8ws) 1 % Sample Height from Ground Y.~() feet Comments: Stack Din. 16 Rdercnce 0 I)orls arc 57" Upstream Irom next disturbance POlt~ arc 468" Downstn,~am from last disturban~e Traverse Pel"cent Distance From: Ports Point Diameter ID Reference A B C D E F I 4A 0.70 0 .70 101 ·1'2Q 2 14.6 2.34 2.34 ··~.lO 3 29.6 4.74 4.74 ,."( • tj:t. 4 70A 11 .26 11 .26 :}Q .,~' 5 85A 13.66 13.66 <F5"'. ~& 6 95.6 15.30 15.30 1'-f .11' -- Averages: Ts L Flow ---- I.W ~SP ----. L.. Flowl ~p - KEY=> Field Data Sheet Plant: Denison Mines Dale: Z. /'2. q ( ( L- Traverse Tim~ DGM Pomt Clock Min (8) tn', A 1 8:e.e 0 fooO['<1 0 \ 2 1° &1&,3'-0 3 1'0 (.,Z"'~,\.,\(' 4 )1{) ~3t,'-{<.')~ 5 10 f..,'-kl.-n.--)' 6 50 (..i'1 '~i/ B 1 9',l') ~o ~:)'7 -ICf"1- 2 70 (.r.y ,e-5 0 3 1?o {.. (C> 'Cj ~o 4 '110 (."T).'{ {O 5 too ~ <6 ~ ''18'0 6 \~O ~ql, ~Z.5 to'-\~ \ '2-0 10(). 01 { II Total qo. ~ \0 Avera!!.:: COmmltlllS Time 8aghouse Ll.P -e ', tl \·7 e ~~ 1. Lb ~ '.51 !: 1 (4 fLtl > 1 ~ 1 t \ i l . /' TETCO Filter_~,8':1 __ Sample BOX __ ~ __ _ L\P L\H IInH,O) Vacuum unir:(')· Desired Actual (mHp.l .2:~ ~ .D't 1. o~ 3 ~-z..3 \ .f of i.i) 2> 11.1 (·3( L')-.( '1 '''i.'0 1-.01-Z'l:>"Z-.3 .~\ i \-{1 L57 'i ,2" l,-.,~ I.t'J(., y ·1..0 Lot L-:>l 3 .\w\. ~i\ .... n .3- <Ii ",t III ;) ;"-( t.() <0 l ·o~ 3- ; 3\ 1. 51-t, 1':=r d "- '33 ! d.t-\.,,::q... 'i s. 9~2(/ \'7.-l-1 J • '-\9(,/6 ---" \. .1..13 Time 8aghouse ~p 't >{4 Llrt Location' North Yellowcake Dryer Baghouse Operator. iv\'~ ~ ~v.. s-~r~_ Temperatures ,:~. Stack (,T,) Probe Probo Out Filter HllueHi (..fQ 210 l,<3o 211 0 L1i ,0 2L\.( 2.11 271 LiB '1-0 L70 2.11 7..7) ~9 1-\ 2..10 21--) 27-)-25 !l. 270 1.("1 Z{-S' ~O "'2.-'lAO 1.'1;-1..,'0(' (Pt) 11.-Z, t <{ Z7i{ Z"1'f 55 7'?.-LID l'-o) 'V,p) 55 13 ~, t 70 t7-c 5, -it.{ 2(.,.0 Z b't 2.(.::'1 55 Itt 2...(,,( ~2.. t<o 7..-5 'i I) z.~(, Zfo t-{O 55 I , (j6~ ~ 1 ( . '1 1 e",lfe.l7 DGM Temp (T"1.1 Out In 72-72- '7'1 17 78 8~ ~z.. q3 g-)' (00 S~ io3 '9 0 '18 <7' '2..-11' ~~ Cj9 G:' .'{ !()o ~) 103 1(, 10 (' Ltl( ~o.~ Page _~ _0c.1___ Run !'! _~_ r B AD N Stae!" Diameter 16" Port Reference _0,0" Ports are 57" Upstream from next disturbance Ports are 468" Down~tream from last disturbance Assumed Moisture ~(O ---- Probe L!6..i:2. Cp 0,84 Nozzle Calibration .11(7 ·2 'f0 ·2 t 1-2 '..-1 • 1" r v-/ Avg Dn ~ 2 ~ ~lcbes Gas Bag Ambient Air Console :> ---- Y-Factor {, ooi 6H@ i' 't(<..{ ~il H20 Barometric Pressures Pb", __ ? t.j_·Jz"f~ __ in Hg Pb. 2 ~ -'-{ 3 in Hg I .-, -----... -.. ---".,,---~ p(. ____ -_~L.\. ___ inH;O Leak Ch~ck Pre H"!l1ltn D-oottJ \"ac Llll-ig ZI- PltOI Ra(~ D-O Ir;H,O ~ Water Collected Time Salllpic::d RCVle\\ K K - Post 0 '003 t? ___ ~_!._.oo ~ ,..;, ~/ 1\J \1.10 ,~ /iJT", rcrr " '" mill North Yellow Cake Scnlbber Sample Recovery Gas Analysis Data (ORSAT) Ye110w Cake Dryer Baghouse Sample Recovery Gas Analysis Data (Ambient) Chain of Custody Lab Analysis APPENDIX C c METHOD 5 Facility: Denison Mine Stack Identification: NYC Scrubber ~~~~~--------------------------- I.MPINGERS ~";'lJrtt ~~ 5B~~ 5~~7 IMPINGERS IMPINGERS IMPINGER~ Final (g) Initial (g) Net (g) Run: \. Sample Box: A lmpinger Number --- Initial Volume ofliqui(\ (H20) in impingers, (ml) drop out I 100 I 100 I SilicaGe! 5 " q~\{.1(p ljte'i ~1..~;L ~qtlbO Ct> 09 ~:~ q'io.t) 5(.x,,,~ frj (. '"1 51 1 '(1 ~:Sf). ~ ~(;!"'l, c1 8~<tb { ~ '1 ',,\~:) ?.i),':f-~f·.) \,~~t.{ ~.~ S<J.5 Total (g) "7 0 ~. ~ ========= Run: Z--Sample Box: /i ---'-~- fUlplnger NUmber db 2-I 3 I 4 I l ..i., Initial Volume of liquid (H20) in impingers, (ml) drop out I 100 I 100 I [ Silica 0iliLJ ___ 6 __ 7Z0. r ~1.[ Total (g) S i) "".{J ======== Sample Box: ___ _ Run: -----......... """""" ......... ---"""""iflm....,...,p""i'j .... n .... g-er""""'l!f'N'F'u .... m"""l"'b"""er----... ••• • 2 I 3 I 4 I .L [ ~ Initial Volume ofliquid (H20) in impingers, (ml) drop out I 100 I 100 I r Silica Gel F~~~)~~~j ~[~ Initial (g) ------~-------+-------+------~----~~,-------Net (g) ======*======b========================== Total (g) ======== Run: ---Sample Box: Impinger NUDlber II..l....I-LI..J....[-L Initial Volume ofliquid (H20) in impingers, (ml) drop out I 100 I 100 I Final (g) ------~-------+-------+------~-------~-------Initial (g) -------+-------+------~-------!-------~.---...---Net (g) ========================================== Total (g) ======== Location_N Y L_, ______________ _ Analytical Method _____________ _ Date 2/ZiLt £, Gas Actual Reading Test No. -J Gas Bag No. :if ijG--..3> CO2 Ambient Temp ~ Operator~ Date zkc..b-v Test No. I~ Gas Bag No. r~c" Ambient Temp "tE Operator Date -----Test No. ___ _ Gas Bag No. ___ _ Ambient Temp ____ _ Operator ____ _ Gas CO2 O2 (Net is Actual O2 Reading Minus Actual Gas O2 (Net is Actual O2 Reading Minus ActuaJ COl 2 .ff Actual Rt'ading Net Actual t .2f '2·r I Ut<t.3 .4~- t02 was detennined using a gas analyzer CO is not measured, as it has the same molecular weight as Nz ?,.fj-2·Y Average Nel Net Net -2·Jr- 1~43 Net Volume Average Net Volume Z dy J ~ .:> Average Net Volume Yellow Cake Dryer Baghouse NY C Baghouse !viS Facility: Denison Mines Date: 1.[ "'loA I i 2 ... Stack Identification: ...:...N.:....;Y:.-:C=--=.B.:.:.iag~h....:.o.:..:.us=-e _____________ _ IMPINGERS r:lt~l-~ 5f1roSV' IMPINGERS 1M PI NG..ERS Final (g) Initial (g) Net (g) Sample Box: .6 --"""'---Run: ---- lnlpinger Number 1.2...14nli Initial Volume ofliqllid (H20) in impingers, (ml) 100 100 I I Silica Gel I 5 Cf4 .~ ~I~·S 5~O·1 l~S{ . .5 ~/B·3 'o3 ·~ 5 "Le{, q e~~,~ ""2.!>\~ 10,' j.8 ~ t? q'Z..,.. Total (g) ================ Run: ----Sample Box: ___ _ ImPinger Number ... L ~ I 3 I ~ I _~ . Initial Volume of liquid (H20) in impingers, (1111) 100 100 I I Silica Gel I I Total (g) ======= Run: ----Sample Box: ---- ~ I ~ I 4 I ~ Initial Volume ofliquid (H20) in impingers, (ml) 100 100 I I Silica Gel I I Final (g) ____ -I-___ -I-___ -+-___ -I-____ ~ Initial (g) Net (g) ============================================ Total (g) ================ Sample Box: Run: ---- hnpinger Nuan6er _ ........ 131.4.=I~.L 6 == Initial Volume of liquid (H20) in impingers, (ml) 100 100 I I Silica Gel I Final (g) ~ Initial (g)_= __ +-__ -;-__ -+-__ -+___ _ Net (g) ======================================:====== Total (g) ======= SOC No. Order No. 44698 TestAmerica rptSTLRchTitlt> v3.73 TcstArnerica L.aboratories. Inc. Analytical Data Package Prepared For DenisOll Mines (USA) CorpB Denison Mine 2012 1st Quarter Radiochemical Analysis By TestAmerica 2800 G. Jv. Wayy Richland Wa, 99354, (509)-375-3131. Assigned Laboratory Code: Data Package Contains 15 Pages Report No.: 51178 Results in this report relate only to the sample(s) analyzed. Client SampJe J 0 (List Order) Lot-Sa No. "Vork Order Report DB 10 5865 R1 BAGHOUSE J2C060468-'1 MQ9E31AA 9MQ9E310 FILTER AND BE 5866,5867 R1 NYC J2C060468"2 MQ9E72AA 9MQ9E720 FILTERS AND B 5868,5869 R2 NYC J2C060468-3 MQ9FA2AA 9MQ9FA20 FILTERS AND B BaH'h No. 2067114 2079130 2079130 nit: LE.A(lEF~ IN ENVtRONMENTAl TESTiNG Certificate of Analysis March 30, 2012 Denison Mines (USA) Corp 1050 17th Street. Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab Project Name Sample Type SDG Number L Intmduction March 6, 2012 Denison Mine 2012 1 st Quarter Three (3) Stack Filter Samples 44698 CASE NARRATIVE On March 6,2012, three stack filter samples were received at TestAmerica's Richland laboratory for radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification numbers as described on the cover page of the Analytical Data Package report form. The samples were assigned to Lot Numbers J2C060468. H. Sample Receipt The samples were received in good condition and no anomalies were noted during check~in. HI. Analytical Results/Methodology The analytical results for this report are presented by laboratory sample 10. Each set of data includes sample identitication information; analytical results and the appropriate associated statistical uncertainties. The analysis requested was: Alpha Spectroscopy Uranium-234, -235, -238 by method RL-ALP-004 IV. QuaJity Control The analytical result for each analysis performed includes a minimum of one laboratory control sample (LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Comments" section. 'fest A me rica Laboratories. Inc. 2 Denison Mines (USA) Corp March 30, 2012 V. Comments Alpha Spectroscopy Uraniurn-234, 235, 238 Samples 5866, 5867 R I NYC and 5868, 5869 R2 NYC initially failed due to smeared spectra. The re- analysis is within acceptance criteria. The achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to historical process knowledge. The sample activity exceeds the MDA and detection limit for three of the four samples. The batch blank activity also exceeds detection limit; however, the blank results are significantly lower than sample results. Data is accepted. Except as noted, the LCS, batch blank, sample and sample duplicate results are within acceptance limits. [ certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically and for completeness, for other than the conditions detailed above. The Laboratory Manager or a designee~ as verified by the following signature has authorized release of the data contained in this hard copy data package. Reviewed and approved: Erika Jordan (~~~) 2012.03.30 16:52:16 -07'00' ---------Erika Jordan Customer Service Manager ·restAmcricn Laboratories, [nc. 3 Drinking Water Method Cross References DRINKING WATER ASTM METHOD CROSS REFERENCES I Referenced Method lsotope(s) Tes1America Richland's SOP N EPA 901 .1 Cs-134,1-131 RL-GAM-001 EPA 900.0 Alpha & Beta RL-GPC-001 EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002 EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002 EPA 903.1 Ra-226 RL-RA-001 EPA 904.0 Ra-228 RL-RA-001 EPA 905.0 Sr-89/90 RL-GPC-003 ASTM 05174 Uranium RL-KPA-003 EPA 906.0 Tritium RL-LSC-005 Results in this report relate only to the sample(s) analyzed. Uncertainty Estimation TestAmerica Richland has adopted the internationally accepted approach to estimating uncertainties d(~scribed in -'NIST Technical Note 1297, 1994 Edition". The approach, "Law ofPropagatioll of Errors". involves the id(:~ntificati()n of all variables in an analytical method which are used to derive a result. These variables are related to the analytical result (R) by some functional relationship, R = constants * t1x,y,z, ... ). The components (x.YJ) are evaluated to determine their contribution to the overall method uncertainty. The individual component unceltainties (ut) are then combined using a statistical model that provides the most probable overall uncertainty value. All component uncertainties are categorized as type A. evaluated by statistical methods. or type t3. evaluated by other means. Uncertainties not included in the components, such as sampJe homogeneity, are combined with the component uncertainty as the square root oCthe sum-of-the-squares oCthe individual uncertainties. The uncertainty associated with the derived result is the combined uncertainty (u,,) multiplied by the coverage factor (1,2, or 3). When three or more sample replicates are llsed to derive the analytical result, the type A uncertainty is the st.andard deviation of the mean value (Sf? n), where S is the standard deviation of tile derived results. The type B uncertainties are all other randorn or non-random components that arc not included in the standard deviation. The derivation of the general It Law or Propagation of Errors" equations and specific example are available on TestArnerica rptGcllcrallnfo v3.72 TestAl1lerica LaboratOlies. Inc. 4 o. Report Definitions 1--Actio~T';;--~!---------An agreecf'Jp<;nactT~-ityTe~ef~~sed io trigger some acti()n when the flnaTre:~t~fiis g~{~ate;:-lf{;l~l-~);:-·~;(i~;-;Ii-I(;·tiic-~\(;-t;o;;--- i Level. Often the Action Level is related to the Decision Limit. Batch Bias COCNo Count ErrOl' (#s) TotallInccrl (#s) u(._ Comhined Ut1certain~v. (#s), Coverage Factor CRDL (RL) Lc MDqMDA Primary Detector (~ati() U-234/{l-238 , RstJMDC Rstffotlicert , Report DB No RER SDC Sum Rpt Alpha Spct Rst(s) Work Order Yield The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed together. Defined by the equation (Result/Expected)-I <L<; defined by ANSI N 1330. Chain of Custody Number assigned by the Client or TcstAmerica. Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the samc units as the result. For Liquid Scintillation Counting (LSe) the batch blank COLint is the background. All known uncert.ainties associated with the preparation and analysis of the sample are propagated to give a measure of the ullcertainty associated with the result. 11, the combined uncertainty. The uncertainty is absolute and in the same units as the result. The coverage factor defines the width oCthe confidence interval, I, 2 or 3 stancl,mi deviations. Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmerica "def;:ntlC nominal detection limit. Often referred to the reporting level (RL) Decision Level based on instmment background or blank. adjusted by the Efficiency, Chemical Yield. and Volurne a:ssocia\cd with the sample. The Type I error probability is approximately 5%_ Lc=( 1.645 '" SqJ1(2*(BkgrnclCntIBkgrndCntMin)/SCntMin)) * (ConvFeti(Eff-leYld*Abn*Vol) * IngrFct). For LSC methods the batch blank is used as a measure of the background variability. Lc cannot be calculated when the hackground count is zero. -flle number assigned by the UMS software to track samples received on the same day f(lr a given client. 'The sample number is a sequential number assigned to each sample in the l.ot. Detection Level based on instrumenl background or blank, adjusted by the EHiciency. Chemical Yield, and Volume with a Type I and II elTor probability of approximately 5%. MDC = (4J)) * Sqrt(BkgrndCnUBkgmdCntMin)/SCntMin) + 2.71 /SCntMin) * (ConvFct/(Eff* Yld '" Abn * Vol) '. IngrFcl)_ For LSC methods the batch blank is used as a measure of the background variability. The instrument identifier associated with the analysis of the sample aliquot. The U-234 result divided by the U-238 result. The LJ-234/U-238 ratio for natural uraniulll in NIST SRM 4321(' is 1.038. Ratio of the Result to the M DC. A value greater than I may indicate activity above background at a high level or confidence. Caution should be used v"'hen applying this k'lctor and it should be used in concert with the quuli fiers associated with the result. Ratio of the Result to the Total Uncertainty. lfthe uncertainty has a coverage factor of2 a value greater than I Illay indicate activity above background at approximately the 95% level of confidence assuming a two-sided conlidence interval. Caution should be used when applying this f~lctor and it should be llsed in concert with the qualifiers associated with the result.. Sample Identifier used by the report system. The number is based upon the first five digits of the WOI'k Order' Number. 'nlC ~quation Replicate Error Ratio = (S-D)/[sqrt(TPUs2 + TPUd~)] as defined by {CPT BOA where S is the original sample result, D is the result ofthe duplicate, TPUs is the total uncertainty of the original sample and TPUd is the totalunccrta.inty of the duplicate sample. Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt. The sum of the reported alpha spec rt'sults t()f tests derived from the same sample excluding duplicate result \-vhcrc the results arc in the smne units. The LI MS software assign test specific identifier. TIle n;covcry orthe tracer added !o the sample such as Pu·242 used to traee a Pu-239!40 method. i .. -.----~-::;.:::-:~ ~-.--===== -.:=:==-=--===--::-.:-".-====._=._-=:._----::;::--===== .-.~ ._-_.. -_7:'::::::':'::=::':'::::::·_'".:7.:::=:.:'::::.·'::~.:._·::::::''':::::::'::':::::::_. __ :;-:.:::::::.-~. TestAmerica l-ptGcneralInfo \'3.72 TestAmerica Laboratories. Inc. 5 Sample Results Summary TestAmerica Ordered by Method, Batch No., Client Sample 10. Report No. : 51178 Client Id Batch Work Order Parameter 2067114 FFSR 5865 R1 BAG HOUSE FILTER AND BE M09E31AA U-234 2079130 FFSR U-235 U-238 5866,5367 R'I NYC FILTERS AND B MQ9E72AA U-234 U-235 U-238 Result +-Uncertainty ( 25) Qual Units 5.30E-04 +-1.4E-04 UCI/SA 2.60E-05 +-2.7E-05 U UCIISA 7.29E-04 +-1.8E-04 UCI/SA 3.73E-02 +-6.5E-03 UCI/SA 1.00E-03 +-5.3E-04 UCI/SA 3.85E-02 +-67E-03 UCI/SA Date: 30-Mar-12 SDG No: 44698 Tracer Yield 82% 82% 82% 101% 10'1% 10'1% MDL 2.67E-05 2.67E-05 2.67E-05 4.01 E-04 3.04E-04 4.36E-04 CRDL RER2 9.00E-iS 9.00E-i5 ,)1),"[ 9.00E-15 9.0DE-i5 9.00E-15 , .. ! (, 9.00E-15 \) 5868,5869 R2 NYC FILTERS AND B M09F A2AA U-234 U-235 . 4.73E-02 2.01 E-03 +-8.0E-03 UCI/SA +-7.7E-04 UCI/SA 99% 3.47E-04 9.00E-15 Ie/1ft \ ~ 99% 2.94E-04 9.00E-15 U-238 4.48E-02 +-7.6E-03 UCI/SA 99% 2.94E-04 9.00E-15 No. of Results: 9 RER2 -Replkat(' l~rr()r Ratio:: (S·J))!(sql't(sq(TPUs)+sq(TI)l)d))l as defined by ICPT BOA, T estAmerica rptSTLRchSaSum mary2 V5.2.18.2 A2002 t' Qual -Analyzed for bllt not ddt'cted above Iimitillg criteria. limit criteria is less tb~1II tbe Ml1dMd~IJMdl, Total I )111"{'.-I. CRDL RDt Or' not. idi.'lItified by gamma scan software. TestAmcrica L.ahoratories, Inc. () QC Results Sumuaary Date: 30-Mar-12 TestAmerica Ordered by Method, Batch No, QC Type" Report No. : 5'1178 SDG No.: 44698 Batch Tracer LCS Work Order Parameter Result +-Uncertainty ( 25) Qual Units Yield Recovery Bias MDL FFSR 2067114 BLANK QC, MQ97N1AA U-234 2.1BE-OB +-2.7E-OS U UCI/SA SO% 3.50E-08 U-235 O.OOE+OO +-1.5E-OB U UCI/SA 80% 3.09E-08 U-238 3.71E-08 +-3.5E-08 UCIISA 80% 3.50E-08 2067114 LCS, MQ97N1AC U-234 1.03E-06 +-2.SE-07 UCIISA 84% 104% 0.0 3.78E-OS U-238 1.04E-06 +-2.8E-07 UCI/SA 84% 100% 0.0 3.05E-08 FFSR 2079130 BLANK QC, MRG9V1AA U-234 -1.61 E-12 +-1.3E-OS U UCI/SA 94% 4.44E-08 U-235 -1 .21 E-09 +-'1.2E-08 U UCI/SA 94% 2.89E-08 U-238 -2.41 E-09 +-1. 3E-08 U UCI/SA 94% 3.41 E-08 2079130 LCS, MRG9V1AC U-234 8.51E-07 +-2.3E-07 UCI/SA 97% 86% -0.1 3.00E-08 U-238 1.04E-06 +-2.7E-07 UCI/SA 97(% 100% 0.0 300E-08 No. of Results: 10 TestAmerica mas -(nesllItlExpected)-1 asdcf'incd by ANSI NI3.30. rptSTLRchQcSum Ii Qua! -Analyzed for but not ddected above limiting criteria. Limit criteria is less thall tbe Mdc/MdlllMdl, Totall.i!lccrt. nun .. RDL 01' mary V5.2.18.2 not identified by gamma scan softwarr. A2002 TestAmerica Laboratories, Inc, 7 lab Name: TestAmerica lot-Sample No.: J2C060468-1 FORM I SAMPLE RESULTS SDG: 44698 CHent Sample 10: 5865 R1 BAGHOUSE FilTER AND BE Denison Mine 2012 1st Quarter Report No.: 51178 coe No.: Parameter Batch: 2067114 U-234 U-235 U-238 No. of Results: 3 Result FFSR 5.30E-04 2.60E-05 7.29E-04 Comments: Count Qual Error ( 2 s) 1.2E-04 U 2.7E-05 1.4E-04 Total MDL, Rpt Unit, Yield RstlMDl, Uncert( 2 s) Action Lev Lc CRDL(RL) RstfTotUcert Work Order: MQ9E31AA Report DB 10: 9MQ9E310 1.4E-04 2.67E-05 UCflSA 82% (19.9) 4.36E-06 9.00E-15 (7.3) 2.7E-05 2.67E-05 UCI/SA 82% 0.97 4.36E-06 9.00E-15 (1.9) 1.8E-04 2.67E-05 UCf/SA 82% (27.3) 4.36E-06 9.00E-15 (8.1) _ .. ,---_._. __ ._ .. __ ._-_ .. _--_.- Ratio U-2341238 = 0.7 Date: 30-Mar-12 CoUection Date: 2/29/20128:00 :00 AM Received Date: 3/6/2012 11 :30:00 AM Matrix: FILTER Ordered by Client Sample 10, Batch No. Analysis, Prep Date 3/14/1207:41 P 3/14/1207:41 p 3/14/1207:41 P Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.00109 Sample 0.00109 Sample 0.00109 Sample Primary Detector ALP219 ALP219 ALP219 TestAmerica MDCIMDA,Lc -Detection, Decision Level based 011 instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDl, RDl or not identified by gamma scan software. V 5.2.1 8.2 A2002 TestAmerica Laboratories. Inc. 8 Lab Name: TestAmerica Lot-Sample No.: J2C060468-2 FORM I SAMPLE RESULTS SOG: 44698 Report No. : 511 78 Client Sample iD: 5866,5867 R1 NYC FILTERS AND B Denison Mine 2012 1st QUarter coe No.: Parameter Batch: 2079130 U-234 U-235 U-238 No. of ResuUts: 3 Result Count Qual Error ( 2 s) FFSR 3,73E-02 3.1 E-03 1.00E-03 5.1 E-04 3,85E-02 3,1 E-03 Comments: Total MOL, Rpt Unit, Yield RstlMDL, Uncert( 2 s} Action Lev lc CRDl(Rl) RstlTotUcert Work Order: MQ9E72AA Report DB 10: 9MQ9E720 6.SE-03 4,01 E-04 UCI/SA 101% (93.) 1,14E-04 9.00E-15 (11,4) 5,3E-04 3.04E-04 UCIISA 101% (3,3) 6.60E-05 9,00E-15 (3,8) 6,7E-03 4,36E-04 UCf/SA 101% (88.4) 1.32E-04 9,00E-15 (11.5) Ratio U-2341238 :: 1.0 Date: 30-Mar-12 Collection Date: 2/28/20127:30:00 AM Received Dale: 3/6/2012 11 :30:00 AM Matrix: FILTER Ordered by Client§ample_ID,_Batgh f\{o. __ Analysis, Prep Date 3/26/,12 11 :29 a 3/26/12 11 :29 a 3/26/12 11 :29 a Total Sa Size 1,0 Sample 1,0 Sample 1,0 Sample Aliquot Size 0,0001 Sample 0,0001 Sample 0,0001 Sample Primary Detector ALP7 ALP7 ALP7 TestAmerica MDC/MDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U QUai· Analyzed fot but not detected above limiting criteria. limit criteria is less than the MdclMdafMdf, Total Uncert, CROl, ROL or not identified by gamma scan software, V5,2.18.2 A2002 TestAmerica Laboratories. 1m:. 9 lab Name: TestAmerica lot-Sample No.: J2C060468~3 FORM I SAMPLE RESUL T5 SDG: 44698 Client Sample in: 5868,5869 R2 NYC F!L TERS AND B Denison Mine 2012 1st QUarter ReportNo.: 51178 coe No.: Parameter Batch: 2079130 U-234 U-235 U-238 No. of Results: 3 Resu!t Count Qual Error ( 2 s) FFSR 4.73E-02 3.4E-03 2.01E-03 7.0E-04 4,48E-02 3.3E-03 Comments: Total MDL, Rpt Unit, Yield RsUMDL, Uncert{ 2 s) Action Lev lc CRDL(RL) RsUTotUcert Work Order: MQ9FA2AA Report 08 10: 9MQ9FA20 8.0E-03 3.4 7E-04 UCl/SA 99% (136.4) 9.02E-05 9.00E-15 (11. 8) 7.7E-04 2.94E-04 UCI/SA 99% (6.8) 6.38E-05 9.00E-15 (5.2) 7.6E-03 2.94E-04 UCI/SA 99% (152.4) 6.38E-05 9.00E-15 (11.7) -------_._--_._"_. Ratio U-2341238 = 1.1 Date: 30-Mar-12 Collection Date: 2/29/20127:30:00 AM Received Date: 3/6/2012 11 :30:00 AM Matrix: FILTER Ordered by Client Sample lOr Batch No. Ana~ysjs, Prep Date 3/26/12 11 :29 a 3/26/12 11 :29 a 3/26/12 11 :29 a Total Sa Size 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.0001 Sample 0.0001 Sample 0.0001 Sample Primary Detector ALPS ALP8 ALP8 TestAmerica MDCIMDA,lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTlRchSample U Qual· Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/MdJ, Total Uncert, CRDL, RDL or not identified by gamma scan software. VS.2.18.2 A2002 TestAmerica Laboratories. Inc. 10 FORMH Date: 30-Mar-12 BLANK RESULTS Lab Name: TestAmerica SDG: 44698 Matrix: FILTER Report No. : 51 178 Count Total MDl, Rpt Unit, RstlMDL, Analysis, Total Sa Aliquot Primary Parameter Resu!t Qual Error ( 2 s) Uncert( 2 s) Lc CRDL Yield RsVTotUcert Prep Date Size Size Detector Batch: 2067114 FFSR Work Order: MQ97N1AA Report DB 10: MQ97N1AB U-234 2.18E-08 U 2.7E-08 2.7E-08 3.50E-08 UCI/SA 80% 0.62 3/14/1207:43 P 0.21 0.21 ALP222 7.14E-09 9.00E-15 (1.6) Sample Sample U-235 O.OOE+OO U O.OE+OO 1.5E-08 3.09E-08 UCIISA 80% O. 3/14/12 07:43 p 0.21 0.21 ALP222 5.05E-09 9.00E-15 O. Sample Sample U-238 3.71 E-08 3.4E-08 3.SE-08 3.50E-08 UCI/SA 80% (1.1 ) 3/14/1207:43 P 0.21 0.21 ALP222 7.14E-09 9.00E-15 (2.1 ) Sample Sample Ratio U-2341238 = 0.6 _____ , ••••• _ •• ____ ._." __ " __ HH •• ' ________ H __ " __ H_._ •• __ • ________ ,._. __ .H ___ ._._" •• ____ ••• _______ ••• __ • ______ •• _ ••• --_H. __ ._~ •... _ .. ,,_ ... _. ___ " __ .• _. ___ •. __ .. _ ... ____ .. _. _______ .... _._._._ ....... _ ..•..• _ ••.. _ ............ __ •. _ _ .... __ ._. __ ....... _.- Balch: 2079130 FFSR Work Order: MRG9V1AA Report DB iD: MRG9V1AB U-234 -1 .61 E-12 U 1.3E-08 1.3E-08 4.44E-08 UCIISA 94% O. 3/26/12 11: 31 a 0.23 0.23 ALP9 1.40E-08 9.00E-15 O. Sample Sample U-235 -1.21 E-09 U 1.2E-08 1.2E-08 2.89E-08 UCI/SA 94% -0.04 3/26/1211:31 a 0.23 0.23 ALP9 6.27E-09 9.00E-15 ~0.2 Sample Sample U-238 -2.41 E-09 U 1.3E-08 1.3E-08 3.41 E-08 UCI/SA 94% -0.07 3/26/12 11:31 a 0.23 0.23 ALP9 8.B7E-09 9.00E-15 -0.38 Sample Sample Ratio U-2341238 :;;; 0.0 ._-----. __ . __ ._----------------._-_ ... _----_._._ .. _-_.-------.---.----.--------------... --.-.- No. of Results: 6 Comments: TestAmerica MDClMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTlRchBlank l! Quai -Analyzed for but not detected above limiting critrria. Limit criteria is less than the Mdc/Mda/Mdl. Total Uncert, CRDL, RDL or not identified by gamma SCHIl software. VS.2.18.2 A2002 -resLAmerica Laboratories. Inc. 11 Lab Name: TestAmerica Matrix: FILTER Count Parameter Result Quai Error ( 2 s) Batch: 2067114 U-234 U-238 Batch: 2079130 U-234 U-238 FFSR 1.03E-06 1.04E-06 8.51E-07 i .04E-06 1.8E-0? i .8E-07 1.5E-07 1.6E-07 Total Uncert( 2 s) MOL FORM!! Les RESULTS Report Unit Yield Work Order: MQ97N1AC Report DB 10: 84% 2.SE-07 2.8E-07 3.78E-08 UCI/SA 3.05E-08 UCI/SA Rec Limits: 84% Ree limits: Expected Expected Uncert MQ97N1CS 9.86E-07 3.06E-OS 75 125 1.03E-06 3.20E-08 75 125 Work Order: MRG9V1AC Report DB 10: MRG9V1CS 2.3E-07 3.00E-08 UCI/SA 97% 9.SSE-07 3.07E-08 Ree Limits: 75 125 2.7E-07 3.00E-OS UCl/SA 97% 1.04E-06 3.21 E-08 Rec Limits: 75 125 SDG: 44698 Report No.: 51178 l<cconl"Y. Analysis, Bias Prep Date 104% 3/14/12 07:43 P 0.0 100% 3/14/12 07:43 P 0.0 86% 3/26/12 11 :33 a -0.1 100% 3/26/12 11 :33 a 0.0 Date: 30-Mar-12 Aliquot Primary Size Detector 0.25 ALP226 Sample 0.25 ALP226 Sample 0.25 ALP10 Sample 0.25 ALP10 Sample -----------_ .. _------_._----_ •.. _----_._-... _------._ ... __ .... _ ... _-.--_ ..• _._-.-_.-.. -'-.-.--~ ..... _---_. __ .-._---------._------.. _-_._---------~----.... --.---.-.. -.---.-... ---.--... ---.. --... -.-.. ---.. _._-._ .... -_.-.-. ---_ .. _--.. _-----. --_.-.. __ .---------.•.. --... -. No. of Results: 4 Comments: TestAmerica rptSTLRchLcs VS.2.18.2 A2002 Bias -tHesuItiExpected)-l as defined by ANSI M3.30. TestAmcrica Laboratories. Inc. 12 D;'- > ::! ~. ;:0 r ;:0 ~ CJ ~ ~. ~ ! ..... .J ~~~~;t~~~~~~~~j~;::lf~~~t.ti~)it~~~r.~~~~~~i?r~ Chain of Custody Record Temperature on Receipt __ _ TestAmerica Drinking Water? Yes 0 No 0 THE LEADER IN ENVIRONMENTAL TESTING TAl-41N (1007) Ciiont Tetco Address 391 East 620 South City -- American Fork I State I ZiD Code Ut -L 84003 Proiect Name arId Location (State) Denison Mine 2012 1st Quarter Cof11ractIPurch5sa Order/Quaff:! No_ Sample I.D. No. a.nd Description (Containers for each sample may be combin~ on ons line) 586S Rl Baghouse filter and beaker 5866, 5867 R1 NYC filters and beaker 5868,5869 R2 NYC filters and beaker Loi:IJ-J 2.( chO 4 b ~ i[J6 if '-I b c;(t& ~ -q-3-J L Possible H<izard Identif.'CaCion o Non-Hl1Z8rd 0 Flammable o Skin Imlant Date 2/29/2012 2/28/2012 f 2/29/2012 o PoisonS I Profect Manacer I Dean Kitchen i Telephone Number (Area CodeilFax Number I 801-492-9106 Site Contact I Cab Contact S~ott Cnrinc:nsen.,.RV3n P:almt:r CarriorlWa}'bifJ Number Containers & Malrix Preservatives '----TJ ~! I ! ~ I ~ I 8[_ ~ I~a I Time III ~ _ ~ I § ~ €i ~ ;f ~~I ~;oo X I I I I J 7:30 X I I j I I I ! 730 Ix ~ I , ~ " I I I i 1 i +-I I I~ I 1 i I I i I T I I 1 I Sample-Disposal o Unknown 0 Retum To Client ~iSPOS8f By Lab I oi ~l ~! :::> 1-[ t I ~ !X -i X 1 i i f T I I I I 0 H JJ I Chain of Custao'v Number ! Dare 2/29/2012 !.2bNumber I Page of L Analysis (A~ach lisrif morerrrrrm ~I i' I Special fnstructions/ Conditions of Receipt /£1Q c:r 7:-3 I J11& qE '/ r In -T~lm---r/1 Q cr.i/t 1 o Archive For ___ Months (A fee l1".ay be assessed if S<lmpfes are retained fonger than 1 month) Turn Around Time Required QC Requirements (Specify) o 24 HfUS\ 0 48 !!.ours (0 7 Days 0 14 Days 0 21 Days 0 c;rhe~ as per method I' 1_ RBJjn~uish5}jBy --''7'\) ..................... [ _-:-\-. l Date , Tim,e ~ () r ~ ...-r-A-L-rL. j~ -(p -{ :1.! f {,~ 2. ReJinqrJ/s;hed Sy' '-" -r Date-! Tims , Time i 3. Received By I. Date 3. Relinquished 8}' I Time i I Dale Comments When Complete Email to:DeanorPaultetco@tetco-ut.com DISTRI8UTION, wRITE -F1ewmed to Client with Report; CANARY. Stays with the Sampte;PINK -Fieid Copy TestAmerica ~~ THe LEA()!O!l IN ~NVHlONMHI1'AL TESTING S~unple Check-in List Date/Time Received: <~ .~ I....{I -\.k \ \ I 'i-.~ __ . __ Container GM Screen Result: (Airlock) __ ,,"_. D.\Q_ lnitialsl~~] ~ Sample OM Screen Result (Sample Receiving) _______ lllitials[ t" J Client:j) t N _ SDG II-:~ b 14, NA [l SAF #: NA('P Lot Number: j 1-LO b6 ~64~ __ Chain of Custody if "_ .. __ ------. __ ._-------•...... - Shipping Container ID: ... __ . NA\J Air Bill Number: . NA~ Samples received inside shipping container/cooler/box Yes [\> ] Continue with 1 through 4. Initial appropriate response. 1. Custody Seals on shipping container intact? 2. Custody Seals dated and signed? 3. Cooler temperature: 4. Venniculite/packing materials is No [ ] Go to 5, add comment to #16. Yes [ No [ Yes [ No [ ____ oC NA[ Wet [ ~') J Dry\"S 1 Item 5 through 16 for samples. Initial appropriate response. 5. Chain of Custody record present? Yes ~] No [ ] 6. Number of samples received (Each sample may contain multiple bottles): ~ -=~------------- 7. Containers reccivcd:~ 'i. -lb.; \~(L. ') ?:> 't.b.Q..c,\ 'LQ-(" 8. 9. 10. 11. l2. 13. 14. Sample holding times exceeded? Samples have: __ tape __ custody seals Matrix: __ A (FLT, Wipe, Solid, Soil) _____ S (Air, Niosh 7400) Samples: ~ are in good condition __ are broken ___ Other _________ _ -----------------_._------_._---- NA( Yes [ hazard labels ~_appropriate sample labels __ I (Water) ~T (Biological, Ni-63) __ arc leaking No t» ] ___ have air bubbles (Only for samples requiring no head space) Sample pH appropriate for analysis requested Yes [ ] No [ ] NA~ 1 (If acidification is necessary, then document sample ID, initial pH, amount ofHN03 added cfu'cl pH after addition on table overleaf) RPL ID # of preservahve used : _____________________ ... _______ . ______ ..... __ . ________ ... Were any anomalies identified in sample receipt? Yes [ ] No~ ] DesGription of anomalies (include sample numbers): NA'fJ LS-023, Rev. 15,07/11 See over for additional information. T ~stAmerica Laboratories. Inc. 14 lestArnerica ~~l rHE Ll!AOEH iN tNvmONM£:::N1Al TEStiNG 15. Sample Location, Sample Collector Listed on CaC? * *For documentation only. No corrective action needed. 16. Additional Infofmation: _____ _ -----_._ .. _--------------- _ .. _-----_._-_._- [ ] Client/Courier denied temperature check. Yes [~] No [ ] ClienUCourier unpack cooler. Date: ~.-~., \~ Saml)le CuRtodiat~~~ _~-=.=~=. =--:'\.."----__ _ ··C)~------- Client lnforrned oll _________ by ____________ Person contacted ___________ . l )Q'~ 0 ad:i on necessmy; proceRS as is Pn>jecl Manageo. ___ ~.AJM_ q~ Date :3 -1-/2 SAMPLEID Initial pH Acid AmI. Final pH SAMPLEID Initial pIT Acid Amt Final pH ~~~~----~--~---i~~\~\------~--~--~--~ i------'~----_t_----_t_----_+_---__i!I___';-------_t_----_+__----.. -.. ---------, '~ \, ~--~~~---~--~I --~~\--~--~~----- r------'\\~+-----f-----t--____s_---\···--'-::-··,--r__-----j----+__-.. ----\ \\ r_-----------~------~------_+_-----_1~-----------~----~------_r---------------4 \ \ \ \ ,-X~ I ~1{/? f-------------!----=:..--"\N,O~----t------i------------l...Ji:::T"~'¥-fV~-----+----------1---.-.-------- ~~ ~. ,-----------------1r----------1,~t_----t_---~-----------r_--_'l.::;o>'_-I_-----~--__+-------\ \~ ~ '\f \ j~ ''\ ~. ~/ \ <: --I---------\f-----------------1---------'~-------I_----__j \;( \~. f-----------I-----__I---"\""---t-----li1----~------------ \ -- ~------------~-------1--------__I-----~-------------_+-------_+----~---r----~ : 1\ \ r--------+---I------tl-____ --------j--I--~-.-\f--- l\-__ _ \ -----------------r------r------+------.------, 1_-----------~.---------___1I_--------+------~----------------__+---------+_-----+--~--~ I ~ __________ ~ ______ ~ ______ -L ______ ~L--. _____________ L_ ______ ~ ____ ~ _______ ___ LS-023, Rev. 15,07111 See over for additional illt<:mnatioll. T estAmerica Laboratories_ Inc. 15 APPENDIX D Nmih Yellow Cake Scrubber Figure 1. Facility Schematic Representation Yellow Cake Dryer Baghouse Figure 2. Facility Schematic Representation Process Data (Retained by Denison l'v1ines) o North Yellow Cake Dryer Scrubber Facility Denison \111 lnes t a t y Stack Identification: North Yellow Cake Scrubber 1 -cE-0~1 b i f3 a : Distance upstream from next disturbance, feet 9.5' ------------------- 0: Distance downstream from last distllrbance. feet 9.5' y: Distance of Sample Level to Ground, feet 65 ' 0: Stack Inside Diameter, inches 18" Estimated Moisture, percent 8-1 Y~·'O Estimated Temperature, OF 100-120 ------------------- Estimated Velocity, ~)m 1,100 Control Unit Type: Scrubber Number of POlis 2 ~ Figure I. Facility Schematic Representation Process Type: YeHow Cake Processing Denison Mines Process Data i r Source: North Yellow Cake Date: I / . [, ! lS' JU Scrubber Flow GPM Time #1 #2 /}P '?flOo lj'3 li'3 3· z y,'J tJ L{ ') Ci''C ),7 Cfv'o Q <-t· ") ~--~~ -)' -S ~~ > D y. ~( ~ .. -S '~, L -- lU,'DD C( -3 q -l.( ~,~ --c J ~ 3 D t-f,) )/'3 3·) (It c· D 0 l{ r') ?f' 3 '-5 ' 'Z.. .- ~(; s u Y I ~-> v· J "). ~; (Z,~ ~&> l( . ) «·3 s·j I Z 2 > 0 ct· ) ~ . <; ~·L. i '>; 0 () L-( 7 '1 C(. '7 'S,""S IS: ~ 0 "--( . ) YO) -;. "S (L-(: 0 b L( c) S'L 5·(~ \ L L( '1 '> () y.) i ,-C '),Z l '( ~ UD cA.) )'·2. ~.2 \ t; ; )0 ~\. ~ ~ . "L-'~ ,1> lb: \) D L\. ~ c{, '0 ~.~ \0: ~ 0 c,\. ; fr' \-( ~~ .) Denison IVIine Process Data I / Source: North Yellovv' Cake Date: Z/ZC;/IZ Scrubber Flow GPNI Time #1 #2 6P i--,' 3 () L/. ~ 0·3 S·z If.'Uc) L{ . "7 C\I( 5. -L. ~< -3 0 L(' ~ S·~ .>. L- ~: DO 'v( · <-; q.~ ~ i-c. c:::, : 3 (.) l.--{, ) til . 1-. ~.--S ( V : uo q,) q'L :>' s 10: > D ~/~ V1. "L )') I ( : O() l-( t~ C1. ( --; . z.. t ( r ~ 6 G( I") e,. 1 )I~ / t : ()D ~( ') q.z. '$ , l.-- { Z " ~o C-{ • '7 (/{ .7-, ;,. -z. l> .' 00 ~.) C\. ') 1'~ t ~) : ,0 q.) / vr."-L 7-') \. \...( : OU <-(,t c1'O f-Z t \...( : 50 cl·~ (/1' \ ~t0 / I )"-: DO vbJ 1 '2-. q. rt '). "t-' '\ L>.' 3t> (/( . ~ '1 . 'z, 1·L f &.' 0 c> (y , "'G Gt·f " t- -- Yellow Cake Dryer Baghouse F I:') aci !ity: .:~ I> s s()n. _ Q ~. ."7 if •. ,. .~ ~ ..... r-." .. .-, Q )Ti 1 "'-"" 1r"II Stack IdentIfication: . c; ... 10\r\ ~,-"al(e tla.gholi~t; t a i V / 1~0~1 £ it ~ a: Distance upstream from next disturbance, inches 57" ------------------- [3 : Distance downstream from last disturbance. inches 454·H y: Distance ofSamp[e Level to Ground, feet 65' 16 q 0 : Stack Inside Diameter, inches ________________ _ Estimated Moisture, percent (J_::~J() Estimated Temperature, of p~ ---------------------- Estimated Velocity. fpm 1,400 Controillnit Type: Number of P0l1S '* ., .<'w Figure 2. Facility Schematic Representation .-- Process Type: 1'1,;.:110\\ Cdkc APPENDIX E Calibration of the console dry gas meter(s), pitot tubes, nozzles diameters, and temperature sensors were carried out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 3 Schematic of IVlethod 51114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-test Dry Gas Meter Calibration Data Forms Type S Pitot Tube Inspection Data Sample Box Temperature Sensor Cal1bration E Temperature Sensor ~ ImpingerTrain Optional, May Be Replaced By An Equivalent Condenser ====tl Probe Type S Pitot Temoeraiure T~e S~~or Temperature sensor~ Gooseneck I . I Temperature Sensor -~------ Nozzle Hset Traced ~ ~i!1Bd . / Probe -----". ~ . P \' Glass Filter / nCr Holder TYP,:; ,~itot \l ~ 1 Healed Area I· -=:..::z -7= --r StacK Wall Manometer Temperature Water . sensor W Orifice J, 'r I ! rq , I I I IT ~ H By-pass 'I , l I I -l ! I Valve I '---J.. ) \ i 1[0) ? ) Dry Gas , L ~" '.' I (Meter) \ 0 ;1 Air-Tight ~ ~ ~pump Empty Figure 3 Schematic of Method 511 ] 4 Salnpling Train Vacuum Line J!. Vacuum Gauge ) 1 ______ METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report). for a period of time necessary to achieve a minimum total volume of 5 cubic feeL 4) Record data and information in the cells. YELLOW cells are calculated. CRITICAL ORIFICE SET SERIAL #: '-,-----' K' -,------j FACTOR G G G RUN# [AVG) 0.8137 0.8137 0.8137 0.5317 0.5317 0.5317 _ 0.3307 0.3307 0.3307 12 857.685 12 863.696 12 869.730 13 840.0900 13 845.380 13 850.723 20 800.747 20 806.875 20 812.608 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 863.696 869.730 875.755 845.380 860.723 856.048 806.875 812.608 817.910 6.011 6.034 6.025 5.290 5.343 5.325 6.128 5.733 5.302 75 75 75 75 75 75 68 68 68 89 90 I 98 90 91 I 100 91 91 ! 104 82 85 91 85 87 92 87 89 95 ,-- 75 79 75 79 80 81 80 83 84 100 104 I 107 I 92 95 98 81 84 83 INITIAL DGM AVG 94.25 96.25 98.25 87.50 89.75 92.25 77.50 81.00 82.50 FINAL 25.45 ELAPSED TIMEIMIN) o 5.50 5.50 5.50 EI 7.50 I 7.50 i 7.50 I 14.00 13.00 12.00 AVG (Pb • .) 25.45 2.55 2.55 2.55 1.11 1.11 1.'11 ir.,rmi 4.9075 4.9085 4.8835 4.3541 4.3797 4.3451 5.1272 4.7656 4.3952 2012 Pre-Calibration IF YVARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 1 4.9257 1.004 4.9257 1.003 4.9257 1.009 AVG= t.005 m 4.3890 1.008 4.3890 1.002 4.389Q 1:.!W! AVG= .1J!.Ql W illl1l 1.000 4.7629 0,999 4.3966 1.000 AVG= 1.000 -0.40 1.460 1.455 1,450 1.501 1.494 1.488 1.402 1.393 '1.:189 The follOWing equations are used to calculate the standard volumes or air passed Ihrough the OGM. V" (sid). and the cntical Orifice, V" (stdi. and the DGM calibration faclor. Y. These equations are automatically calculated In the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 1.004:J ('I) (2) (3) I'm ='K, *l'np l:...t:!:IJ'+(\!f f I3.6) Tm = Net volume of gas sample passed through DGM. corrected to stand3rd conditions K, " 17.64 'Him. Hg (Englisfli. 0.3858 'f(lmrn Hg (MetriC) {'L'r, .'fJ /''''1,. >.< (C) t.: '" -;===-.J I wllh !"('!:.l.[ I'm T,,, = Absolute DGM avg. temperature ('R -English 'K -MetriC) =: Volume of gas sample passed through the cntical orifice. corrected to standard conditions T,",c = l;bsoiute ambient temperature ('R -English 'K -Meine) K'.::: Average K" factor from Cnt!~al Onflce Calibration '" DGM calibration factor AVERAGE t.H@ =;'1A48! L\H@= ( 0.75 e)2 ilH (VI1l(stdl\ Vcr{std) Vn• } Temperature Sensors Reference In Out OF OF OF 32 72 203 33 73 202 32 73 202 Pre 20125 console METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFiCES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range, 2) Record barometric pressure before and after calibration procedure, 3) Run at tested vacuum (from Onfice Calibration Report), for a peilod of time necessary to achieve a mlnlmllm total volume of 5 cubic ieet. 4) Record data and Information in the GREEN cells, YELLOW cells are calculated. METER SERIAL #:1-----1 CRITICAL ORIFICE SET SERIAL #: 14535 K' TESTED r------.----ll FACTOR IVACUUM G o G RUN # I (AVG) 0.8137 0.8137 ~ 0.5317 0.5317 ~.5317 0.3307 2 0.3307 0.3307 (in Hg) 10 972.910 10 978.880 ~_1_0_ 984.874 15 956.756 15 962.038 ~ 967.345 19 940.002 19 945.640 19 951.105 USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: 978.880 i 984.874 I 990.8_~~ 96.2.038 967.345 _~~~.l>60 945.640 951.105 956.384 5.970 5.994 6.016 5.282 5.307 5.315 5.638 5.465 5.279 72 72 72 72 72 72 72 72. 72 87 88 94 88 89 95 89 90 95 81 83 88 83 84 90 84 86 92 70 74 76 74 78 81 78 82 85 FINAL AVG (Pbar) 25.45 25.45 ELAPSED ::l TiME (MiN) AVG e 95 95 95 91 [§ 91.75 3.00 92.25 3.00 90 92 94 85.50 § 87.25 1,20 89.00 1.20 81 75.25 0.43 85 79.60 0.43 88 83.25 0.43 4.9091 4.9221 4.9357 4.3645 4.3712 4.3638 4.7375 4.5559 4.3704 2012 Pre-Calibration IFYVARIAnON EXCEEDS 2.00%, ORIFiCE SHOULD BE RECAUBRATED 1 4.9396 1.00S 4.9395 1.004 ~ 1.001. AVG= 1.004 ..(l.D9 4.4014 1.008 ~ 1.007 4.4014 1.009 AVG '" 1.008 0.36 4.7450 1.002 4.5625 1.001 4.380 1.002 AVG= 1.002 -0.27 The iollow:ng EquatiOns are LJsed TO calculace lhe standard volumes of air passea Ihrougtlthe DGM V", (SId) and the cntlcal orITlce \j" (sta) ana tne DGM cali1)ratlo~ lactor Y. TheSe equations are automatically calculated In the spreaClsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 1.00!,.j (1 ) (2) (3) I'm == K," Vm* Pbar / IJ 6} Tm :: Net volume of gas sample passed through DGM. corrected to standard conditions K, ::: 17 EA °Rlin Hg I Englisrt) Q.3858 °Klmm Hg tiVletnc) /' 'Cl' }' =-A: "i !~/)w' '" (C) .J! umi' I C/' '" /'111. "I T", ~ Absolute DGM avg tern perature (OR -English 'K -Metnc) = Volume of gas sample passed through the Critical Orifice, corrected to standard conditions To~." := Aosolule arnDlent temperature lOR -Englrsr'! 'K -Metrlcj K = Average K faCIOr from Crl,'csl Orifice Calibration ::: DGM calibration factor AVERAGE 6H@ =1~1 .616 :J ilH@ = (0.75 e )2 L\H (Vm(std) V cr(std) V", Temperature Sensors Reference In Out OF OF OF 33 33 33 68 57 68 202 202 202 PRE Console #6 Calibration 2012 1.720 1.718 ~ 1.620 1.614 1.609 1.526 1.514 1.503 METHOD 5 DRY GAS METER CAliBRATION USING CRITICAL ORIFiCES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet 4) Record data and information in the GREEN cells. YELLOW cells are calculated. METER SERIAL #: f---=.::.::.=.--j INITIAL CRITICAL ORIFICE SET SERIAL #:1 14538 EQUIPMENT 10 #: Console #5 TESTED VACUUM (in Hg) G:d~ 0.5317 13 0.5317 13 1-- 0.5317 13 704,1020 709.279 709.279 714.472 714.472 720.036 ----- 8, 8:d~ USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: .0 .0 .0 5.177 5.193 5,564 .0 .0 .0 l i Fill 68 63 66 66 70 68 66 69 10 76 68 69 72 76 77 I III D DGM AVG 0.00 0.00 0.00 66.25 70.25 73.50 0.00 0.00 0.00 FINAL AVG (Ph,,) 25.20 25.20 ELAPSED TIME (MIN) 0 §§ ~ 1.10 7.50 1.10 8.00 . 1.10 §§ -~J~t::' Dennision Mines NYC 8aghouse 4,3897 ~ 4.6537 IF V VARIATION EXCEEDS 2.00%, ORIF!CE SHOULD BE RECAUBRATED 1 AVG= 4.3746 0.997 4.3746 1.001 4.6662 1.003 AVG= 1.000 0.00 AVG= 1.542 1.630 1.521 The follOWing equations are used to calculate the standard volumes of air passed through the DGM. V m (srd), and the critical orifice. V Cf (std), and the DGM calibration factor, Y These equations are automatically calculated in the spreadsheet above AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 1.0~O:J (1) (2) {3} Vm,s:d; :::: Kl *' Vm *' !.,bar + (I:!..H /13.6) Tm - Vcr, lid Phar * e =:; K'", JTamb = Net volume of gas sample passed through DGM, corrected to standard conditions K, '" 1764 OR/In Hg (English) 0.3858 "Klmm Hg (Metne) TO' '" Absolute DGM 8vg temperature CR -English OK -Metnc) = Volume of gas sample passed through the Critical orifice. corrected to standard conditions T.mo = Absolute amblem temperature CR . English OK -Metne) K' = Average K' factor from Cntlcal Orifice CalibraTion y VC1(SId) JIm"".!; = DGM calibration factor AVERAGE ~H@ =lm1~53r:J ~H@= 2 ( 0.75 a) 6H (Vm(std» Ver(std) \. Vm Temperature Sensors Reference III Out OF 32 72 203 OF 33 73 202 OF 32 73 202 post test 20125 console METHOD 5 DRY GAS METER CALIBRATiON USING CRITICAL ORIF!CES 1) Select three critical onflces to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice CalibratIon Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information In the GREEN cells. YELLOW cells are calculated. METER SERIAL #; CRITICAL ORIFICE seT SERIAL #: 1-' ___ ---' K' TESTED FACTOR I VACUUM I RUN # I (AVG) (in Hg) 0:§~ 0.5317 12 692.60 699.106 0.5317 12 699.106 704.978 0.5317 12 704.978 710.563 .0 .0 .0 6.506 5.872 5.585 ~-I 69 69 69 I I 64 69 69 69 70 77 70 74 80 Id 77 80 83 G' G:§~ .0 .0 .0 r---r-r--I II USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: INITIAL 0:l AVG 0 0 69.75 74.00 76.75 0.00 0.00 0.00 FINAL AVG(PI>O,l I 25.2~J 25.20 ELAPSED TIME (MIN) e §§ 9.50 1.20 6.50 1.20 8.00 1.20 §§ " ~ Oennision Mines NYC Scrubber 5.4817 ~ 4.6443 IF Y VARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALIBRATED 1 AVG= 5.5359 1.010 4.9532 1.009 4.6618 ~ AVG= 1.008 0.00 AVG= The following equations are used to calculate the standard volumes of air passed through the OGM, V", (std). and the critical orifice, Vor (sid), and the DGM calibration factor. Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 1.008 (1) (2) (3) Vm(Sld) =: K j * Vm * Pbar -r-(bJl 113.6) Tm Pbar * 0 Verts/d) = K'*')Tarnb = Net volume of gas sample passed through DGM. corrected to standard conditions K, '" 1764 °R/in. Hg (English). 0.3858 °Klmm Hg (MetriC) T m '" Absolute DGM avg. temperature (R -English, OK . MeIne) = Volume of gas sample passed through the critlcar orifice, corrected to standard conditions T.mo;; Absolute ambient temperature eR -English, OK -Metric) K' = Average K' factor from Critical Orifice Calibralton Vcr(s'd; y= -= DGM calibration factor Vrn,'td' AVERAGE ll.H@ =\ 1.663 2 l1H@ = (0.75 e) l1H (Vm(std») Vc,(std) Vm Temperature Sensors Reference In Out OF 33 68 202 OF 33 67 202 OF 33 68 202 post test Console #6 Calibration 2012 1.675 1.661 1.653 Gt L _____ ---/r7------·---T -Pl\ 6-~-~=~:'--------t-f'8 i ~-~- Type S Pitot Tube Inspection Data Technician' PI = .l.-\.(;"b ill. ~_~ __ .~~~(2 ___ in (:'1 < 10') (1.1 < IO~ Z s: 0125 in_ \V :; 003125 in W > 3 inch~s Z > V,) inch ((I '= _ .. __ .~. _____ 0 (/.;=---'--- Z= In \Y"" 6t) t-I in W= (0 t--. .....-(.~ In Z= l L "'i4 m ~-; I j= ~S ""L-lli ~~a-r!"'~~~ Tempt~rat\lrG Sensur Cal Ibrat !ol1 _-.~ _____ _ Rd";?fcncc- 15 PA::~PB'? Ct T) pc S Pi lot Tube Inspcdion D,\w, PileI Tub~ Jd,"i1tili(;li:"i1 P~'''~~ ~~ in f>~ = lJ q S In '------.,e-' --""'--,-- Z -, 0 l:::~ in w :::; () 03 125 ill \\' >:; in<.:h':$ z > 3/·~ im:h «: _0 ____ " ___ .Ll_~_ q~ c~_ .. ___ ,S) __ _ P! -" ~"l_ C· ti v: :0 __ 0 ~?_--L.. in \\' =-_~_.:~ _____ . _ in \ in T["fCO Sample Box Temperature Sensor Calibration :;ell ~ 1I.:sa IC~ ea Dale' 12/2911 1 CaJ ibralor: Kawai McNamara Re/crt:m:<: Omcga CU5 12A III II 1:1"5;11' Thermocouple Temperature Temperature Temp. Diff. Unit ID Location Source Reference Sensor or Result (Medium) ("F) ("F) (,F), PiF ~ Water I" I ]3 0 Oven -.) Waler 205 205 0 Probe Out Water 33 I 33 0 Co Water 205 205 0 I Impinger Out. Water 33 II 32 I 1 \Vater 205 203 2 Oven I Water I 33 II 33 I 0 Water 205 206 -I B Probe Out Water I 33 -11 33 I 0 Water 205 2D4 1 Impinger Out Water 33 II .14 I -I Watcr 202 lOO 2 Oven Water ~~5~t 31 ~ 2 Waler 205 0 C Water 33 II 31 I 2 Probe Out Water 20S 20S 0 Impinger Out Watcr I 33 IE-34 I -1 Water 202 201 I Oven Water I 33 II 31 1 2 Water 205 204 1 D Probe Out Water I 33 II 31 -1 2 Water 205 204 I Impinger Out Water I 33 II 34 I -I Water 202 202 0 Ovell Water F~13_ II 34 I -I \Vatcr ~O) 204 1 E Probe Out Water I 33 IF 34 I -\ Water 205 203 2 ImpingeI' Out Water I 33 II 31 I 2 Water 202 200 2 Watcr I '" II 33 I 0 Oven J,} Water 202 2U5 , -.1 F Probe Out Water I 33 II 33 I 0 Water 202 205 -3 Water II '" II 34 I -1 Impinger Out .L) Watcr 202 200 2 '. f'·i~:rj.~'r "" '.' Water C 33 II .,,, I 0 Impinger Out G .1.1 Watt':r 202 200 2 d , Bater I 33 " 31 I 2 Impinger Oul H 202 200 2 Vvater ;~~;" ~I' ImpingeI' Out I Water II 33 II 33 =i 0 Water 202 202 0 ~. ImpingeI' OUI .I Water II 33 31 33 I () Water 202 202 0 lmpinger Out K I Water II 33 II 33 I 0 Water 202 202 () , ~'~A .it:: .. , ,·f.' APPENDIX F The testing f()llowed the same procedures as outlined in previous protocols and tests at this facility. Prepared fo .. : SECOND QUARTER RADIO NUCLIDE EMISSIONS TEST CONDUCTED AT DENISON lVUNES CORPORATION NOR'I1I YEI.lLOW CAKE SCRUBBER YELLOW CAKE DRYER BAGHOUSE BLANDING, UTAH May 15-16,2012 by: TETCO 391 East 620 South Americ:;lnFork, lIT 84003 Pbone (801) 492-9106 Fax (801) 492-9107 fax Denison Mines Corporation 6425 S Hwy 91 Blanding, Utah 84511 Date of Report: July 11,2012 CERTIFICATION OF REPORT INTEGRITY Technical Elnissions Testing Company (TEIeO) certifies that this report represents the truth as well as can be derived by the n1ethods employed. Every effort was made to obtain accurate and representative data and to comply with procedures set forth in the Federal Register. Mike McNamara Reviewer: ~ jIJL~ Date :o:l I \ 'L I \ '1- I -; I Date: 9.,//2/12-.-----/~~7~·~------- ii T ABLE OF CONTENTS Introduction T'est !)urpose ....................................................................................................................... ,. 1 Test Location and Type of Process ...................................................................................... 1 Test Dates ............................................................................................................................. ] Pollutants Tested and Methods Applied .............................................................................. 1 Test Participants ................................................................................................................... 2 Deviations FrOln EPA Methods ........................................................................................... 2 Qu.ality Assurance ................................................................................................................ 2 Sunlmary of Results Etnissioll ReS1.11ts .................................................................................................................. 3 Process Data ......................................................................................................................... 3 Description of Collected Samples ........................................................................................ 3 Discussion of Errors or Inegularities .................................................................................. .4 Percent Isok.il1etics ............................................................................................................... 4 Source Operation Process Control Devices Operation ..................................................................................... 5 Process Representativeness .................................................................................................. 5 Sampling and Analysis Procedures Sampling Port Location ....................................................................................................... 6 Sall1pUng Point Locatioll ...................................................................................................... 6 Salnpling Train Description ................................................................................................. 7 Sampling and AnaJytical Procedures ................................................................................... 7 Qu.ality Assurallce ................................................................................................................ 7 Appendices A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence iii LIST OF TABLES Table I Measured Radionuclide Emissions '" ................................................................................... 3 II Percellt Isokinetics ............................................................................................................... 4 III Sampling Point Location ...................................................................................................... 6 IV Complete Results, North Yellow Cake Scrubber .............................................. Appendix A V Complete Results, Yellow Cake Dryer Baghouse ............................................. Appendix A LIST OF FIGURES Figure 1 Facility Schematic Representation North Yellow Cake Scnlbber ..................... Appendix 0 2 Facility Schen1atic Representation Yellow Cake Dryer Baghollse .................... Appendix 0 3 Schenlatic of Method 5/114 Sanlpling Train ..................................................... Appendix E iv INTRODUCTION Test Purpose This test project was conducted to detern1ine the total radionuclide emissions fi'om the North Yellow Cake Scrubber and Yellow Cake Dryer Baghouse exhausts in terms of Curies per dry standard cubic foot (Ci/dscf). The Grizzly Baghouse was not tested the second quarter as it was not operational. These tests were for lJ-234~ -235, -238, Th-228~ -230, -232, Ra-226, and Pb-21 ° on the North Yellow Cake Scrubber and Yellow Cake Dryer Baghouse. Test Location and Type of Process Denison Mines (USA) Corporation is located about 5 miles south of Blanding, Utah. Uranium ore is processed into yellow cake, which is shipped to other facilities for additional processing. There are two yellow cake dryers with individual scnlbbers. Both dryer enclosures discharge into the Yellow Cake Dryer Baghouse. The Packaging enclosure also discharges into the Yellow Cake Dryer Baghouse. The North Yellow Cake (NYC) dryer was the only operating dryer at t.he time of the test. The South Yellow Cake Dryer is cun-ently not operational. Stack schematics are shown as Figures 1 though 2 in Appendix D. Test Dates All testing was c0111pleted May 15-16,2012. Specific dates and run tilnes are found on the individual field test run sheets. Pollutants Tested and Methods Applied The tests were a determination of radio nuclide emissions in accordance with EPA Method 5/114. Test rill1 filters and front wash residues were sent to Test Arnerica located in Rjchland~ \Vashington for radiol1uclide analysis. Test Participants Test Facility Garren Pahner Scott Christensen David Turk State Agency None TETCO Doug Olsen J efT (rratol1 Mike McNamara Deviations FrOID EPA Methods None Quality Assurance Testing procedures and sample recovery techniques were according to those outl ined in the Federal Register and the Quality Assurance Handbookfor Air Pollution l'v[easuremen! 5'ysfenls. 2 SUivHv1ARY OF RESULTS Enlission Results Table I presents the findings of the test in Curies per dry standard cubie foot. Tables lV -Vl in Appendix A have more detailed test infonnation. Table I. ~leasured Radionuclide Emissions North Yellow Cake Yellow Cake Dryer Run # Scrubber Baghouse pei/dsef pCi/hr pei/elsef pei/hr 316.6 2.013E+07 86.4 1. 1 96E+07 2 318.8 2.432E+07 AVE 317.7 2.223E+07 Process Data The process was operated according to standard procedures. All pertinent process data was available for recording by agency personnel. Scrubber water flow, pressure drop readings (!~p) were recorded and are founel in Appendix D. The Dryer Baghollse pressure drop readings (l\p) were recorded and are found on the test run sheets. Production data will be subn1itted by Denison Mines. Description of Collected Samules The test filters for the NOlih Yellow Cake Scrubber were heavily covered with a gray colored patiiculate. The front washes vvere clear in appearance. The test filters for the Yellow Cake Dryer Baghouse were lightly colored with a gray colored patiiculate. The front wash was clear in appearance. Discussion of Errors or Irregularities None 3 Percent Isokinetic SmnpHng Each of the tests was isokinetic within the ± 10% of 100% criterion specified in the Federal Register. lsokinetic values for each test run are presented in Table II. Tnblc II. Percent Isokinetic Sam g North Yellow Yellow Cake Run # Cake Scrubber Dryer Baghouse 1 98 97 2 98 4 SOURCE OPERATION Process Control Devices Operation All process control devices were operated normally. Recorded scrubber water How, pressure and baghouse 6p readings were recorded and are found on the test run sheets or in Appendix D. Process Representativeness The faciJ ity \vas operated nornlally. Production data was retained by Denison Mines. 5 SAMPLING AND ANALYSIS PROCEDURES SamJ2ling Port Location The inside diameter of the North Yellow Cake Scrubber stack is 18.0 inches. The two, four-inch dian1eter sample port are located 6.3 diameters (9.5 feet) downstream from the last disturbance and 6.3 diameters (9.5 feet) upstream from the next disturbance. Figure I in Appendix 0 is a sche111atic of the stack. The inside diameter of the Yellow Cake Dryer Baghouse stack is 16.0 inches. The two, four-inch dianleter smnple ports are located 28.38 diameters (454 inches) downstream from the last disturbance and 3.56 dianleters (57 inches) upstream fi-om the next disturbance. The sample port locations are depicted in Figure 2 in Appendix D. Sampling Point Location Table III shows the distance of each sampling point fronl the inside waLl according to EPA T\1ethod 1. Each point is lnarked and identified with a wrapping of glass tape and numbered . T'hese points are detef111ined by measuring the distance fro111 the inside wall. Table HI. SaUl Ie Point Location Sample Point 1 2 3 4 5 6 7 8 9 10 11 12 Distance NYC Scrubber 0.58 1.89 6 from InsidevVall 0.70 2.34 4.74 11.26 13.66 15.30 OtlSe S~unpliug Train Description To determine the actual emission rates for this stack, 40 CPR 60, Appendix A, iVlethods 1-51114 were followed. All sampling trains were nlade of inert Inaterials, (Teflon, stainless steel and glass) to prevent interference of the sampled gas and patiiculate. The stack analyzers used to conduct Methods 1-5/114 are constructed to meet the specifications outlined in the CFR. The temperature sensors are K -type thermocouples. Heater, vacuum and pitot line connections have been designed to be interchangeable with all units used by the tester. A 316 stainless steel probe liner was used for the tests. Figure 4 in Appendix E is a sketch of the Methods 5/114 sampling train. Sample boxes were prepared for testing by following the prescribed procedures outlined in Methods 51114. Sampling and Analytical Procedure~ All sampling and analytical test procedures were as specified in 40 CFR 60, Appendix A, Methods 5/114. Quality Assurance All equipment set-up, san1pling procedures, sample recovery and equipment calibrations were can-ied out according to the procedures specified in 40 CFR 60 and the Quality Assurance Handbook/hI" Air Pollution j\.1easurernent Systems. 7 APPENDIX A: Complete Results and Sample Calculations B: Raw Field Data C: Laboratory Data and Chain of Custody D: Raw Production Data E: Calibration Procedures and Results F: Related Correspondence 8 APPENDIX A Table IV Complete Results, North Yellow Cake Scrubber Table V COlnplete Results, Yellow Cake Dryer Baghouse N0111enclature Sample Equations A Symbol Date Filter # Begin End Pblll ~H Y Ym Tl11 --j~p Wtwc Tt Cp Dn CO2 O2 N2 &CO Ymstd Vw Bws (measured) Bws (sallLJ'Med) Bws Xci Md Ms %1 Ts As PG Pbp Ps Qs Qa Vs Curies Crad ERrad TABLE IV COMPLETE RESULTS DENTSON MINES CORPORATION, BLANDING, UTAH NORTH YELLOWCAKE SCRUBBER EXHAUST Description Dimensions Run #1 Run #2 5/15/20 I 2 5/1612012 5930 5933 Titne Test Began 9:44 7:36 Time Test Ended 18:04 16:41 Meter Barometric Pressure In. I-!g. Abs 24.60 24.50 Orific.e Pressure Drop 111. H2O 0.804 1.195 Meter Calibration Y Factor dimcnsit)nless 1.006 1.006 Volume Gas Sampled--Meter Conditions cf 279.077 337.488 Avg Meter Temperatllre OF 85.2 85.9 Sq Root Velocity Head Root In. H2O 0.2153 0.2712 Weight Water Colkctcd Grams 339.6 629.2 Duration of Test Minutes 480 480 Pitot Tube Coefikient Dimensionless 0.84 0.84 Nozzle Diameter Inches 0.3815 0.3815 Volume % Carbon Dioxide Percent 4.80 4.30 Volume % Oxyg.en Percent 13.50 15.20 Volume % Nitrogen and Carbon Monoxide Percent 81.70 80.50 Volume Gas Samp.led (Standard) dscf 224.087 269.859 VO/l1m,) Wat(~r Vapor scf 16.012 29.667 Fraction H20 in Stack Gas (Measured) Fra(;tiolJ 0.067 0.099 Fractioll H20 in Stack Gas (Satnrated) Fraction 0.073 0.\33 Fraction H20 in Slack Gas "* Fractioll 0.067 0.099 Fractioll of Dry Gas Fraction 0.933 0.901 Molecular Wt. Dry Gas Ib,~bmol 29.31 29.30 Molecular WI. Stack Gas lb/lblllol 28.55 28.18 Percent IsokinClic Percent 98.1 98.4 Avg Stack Temperature (oF 97.7 118.0 Stack Cross Sectional Area Sq. Ft. 1.767 1.767 Stack Static Pressure In. Hl) 0.045 0.045 Sample Port Baronlctric Pressure In. J-Ig. Abs 24.53 24.43 Stack Pressure In. Hg. Abs 24.533 24.433 Slack Gas Volumetric Flow Rate (Sid) dsclll1 l.06£+03 1.27£+03 Stack Gas Volumetric Flow Rate (Actual) ctlll 1.468+03 1.89S+03 Velocity of Stack Gas fj)1l1 8.28E+02 1.07E+03 Radiolludides per sample pei 70940.3 86034.8 Concentration of Radiolluchdes pCi/dscf 316.575 318.814 Em.lsslol\ Raie of R~dionuc!ides pCiihr 2.0 13E+07 2.432E+07 * If the measured moisture content is greater thun the saturated moisture level (supersaturated), the saturated moisture value will be used in all ealculations (40 CFR 60, Method 4, Section J 2.1. 7). AVG J07.9 1.17E+03 t.68E+03 9.49E+02 317.694 2.223l~+07 Symbol Date Filter if Begin End Pbm llH Y Vm TI11 ~t.P Wtwc Tt Cp On CO2 O2 N2 &CO VmS1d Vw Bws Xd Md Ms %[ Ts As Pc Pbp Ps Qs Qa Vs Curies Crad ERrad TABLE V COMPLETE RESULTS, PM DENISON MINES CORPORATION YELLOW CAKE DRYER BAGHOUSE Description Dimensions Run #1 Date 5115/2012 5932 Time Test Began 10:17 Time Test Ended 12:21 Meter Barometric Pressure In. I-/g. Ab5 24.60 Orifice Pressure Drop IIl.Hp 1.771 Meter Calibration Y Faclor dimensionless 1.002 Volume Gas Sampled--Meler Conditions cf 98.241 Avg MeIer Temperature "F 78 . .5 Sq Root Velocity He3d Root Ill. H2O 0.5621 Weight Water Collected Gram~ 19.0 Duration of Test Minutes 120 Pitot Tube Coefficient Dimensionless 0.84 Nozzle Diameter Inches 0.2760 Volume % Carbon Dioxide Percent 0.00 Volume % Oxygen Percent 20.90 Volume % Nitrogen and Carbon Monoxide Percent 79.10 Volume Gas Sampled (Stnndard) dst!' 79.777 Volume Water Vapor scf 0.896 Frac.tion H10 in Slack Gas Fraction 0.011 Fractioll of Dry Gas Fraction 0.989 Molecular Wt. Dry Gas Ibflb11lo1 28.84 Molecular WI. Stack Gas lb!lbllloi 28.71 Percellt Isokinclic Perccnt 96.9 Avg Stack Temperature "F 98.8 Stack Cross Sectional Arca Sq. Ft. 1.396 Stack Static Pressure In. H2O -0.21 Sample Port Barometric Pressure [no Hg. Abs 24.53 Stack Pressurc 111. Hg. Abs 24.515 Stack Gas Volumetric Flow Rate (Std) dsdin 2.31 E+03 Stack Gas Volumetric Flow Rate (Actual) cfln 3.01E+03 Velocity of Stack Gas 11)tll 2.16E+03 RadiollUclides per sample pCi 6893.5 Concentration of Radiollllclides pCiidscf' 86.4099 Emission Rate <If R.adioIlllclidcs pCi/hr 1.196E+07 Dryer Baghouse %l = percent isokinetic, percent As = stack cross-sectional area (fe) ASL\P = see "-/L\P MS Nomenclature Btu = unit heat value (British thermal unit) Bws = fraction of water in stack gas CE3 = concentration of particulate matter, back half (gr/dscf,lb/dscf, etc.) Cf = concentration of particulate matter, front half(gr/dscf,lb/dscf, etc.) Cmetal = concentration of metals (ppm, Ilg/ft3, etc.) atomic symbol replaces "metal" CO2 == percent carbon dioxide in the stack gas Cp = pitot tube coefficient (0.84) ex (avg) = species symbol replaces x. Cx (corr) = actual gas concentration corrected to required percent O2 ~H = orifice pressure drop (inches H20) L\H@ = orifice pressure (inches H20) AP = stack flow pressure differential (inches H20) D5 = diameter of the stack (feet) On = nozzle diameter (inches) EA = percent excess air ERB = emission rate of back half particulate (lb/hr) ERr = emission rate of front half particulate (Ib/hr) ERmmBtu == emission rate per mmBtu or ton of fuel etc. ERx = emission rate of compound which replaces x k-fact = multiplier of test point l-.P to determine test point l-.H L == length of rectangular stack (inches) mBtu = thousand Btu Mel= molecular weight of stack gas, dry basis (Ib/Ib-mol) MF == mass of particulate on filter (mg) MFP = mass of particulate matter on filter and probe (mg) mmBtu = million Btu Mp::::: mass of particulate matter in probe (mg) Ms = molecular weight of stack gas, wet basis (g/gmoJ) N2 ::::: percent nitrogen in the stack gas O2 = percent oxygen in the stack gas ,,-/~p = average of the square roots of l-.P (may also be referred to as ASL\P) Pbm ::::: absolute barometric pressure at the dry gas meter (inches Hg) Pbp = absolute barometric pressure at the sample location (inches Hg) PG ::::: stack static pressure (inches H20) P s = absolute stack pressure (inches Hg) Pstd = 8= Qa :'::: Qs = Qw== absolute pressure at standard conditions (29.92 inches Hg.) time of test (minutes) stack gas volumetric flow rate (acfm) stack gas volumetric flow rate (dsefm) wet stack gas std. volumetric flow (fe/min, wscfrn) Ts == stack temperature tF) T std = absolute temperature at standard conditions (528°R) Tt = see 8 Hill = mean molecular speed (cm/s) Vrn = sample volume (ft?) at meter conditions Vmstd ::::: volume standard (dscf), sample volume adjusted to 68()F and 29.92 inches Hg. M5 Nomenclature v s = velocity of stack gas (fpm) Vwe = volume water vapor (sci) at 6SoF and 29.92 inches Hg. W = Width of rectangular stack (inches) Wt\VC = weight of the condensed water collected (grams) Xd = fraction of dry gas Y = meter calibration Y -factor (dimensionless) Method 5 %1 = Vmstd .. (Ts + 460) .. 1039/ (8 .. V s .. Ps .. Xd • D/) ') As = (Ds-/4) " TC Bws = Vw / (Vmstd +Vv.,) CB == MB .. 0.01543 / Vms\d Cr= Mfi)" 0.01543 / Vmstd ex (corr) = ex (avg) • (20.9 ~ desired %02) / (20.9 -actual %02) Deq = 2 .. L .. W I (L + W) On des = "{0.0269 .. (Pbm + 0.0735) / [(Till + 460) .. Cp .. Xd .. "[(Ts + 460) eMs) / (Ps e ~P)]} EA = (%02 -0.5 %CO) / [0.264 %N2 ~ «%02 -0.5 %CO)] ERn = CB " Qs <I 0.00857 ERF = Cf " Qs .. 0.00857 ERmlllBtll == ERx 1 (mmBtu / hr) K-f~lCt = 846.72" On4 .. ~H@ " Cp 2 .. X/ .. Mel II Ps .. (T,n + 460) / [Ms .. (Ts + 460) .. (Pbm + ~H 113.6)] Md = CO2 '' 0.44 + O2 .. 0.32 + N2 "0.28 Ms = (Md .. Xd) + (1 8 co Bws) Ps = Pbp + (PG / 13.6) Qa = Vs " As Qs = Qa" Xd .. Ps" Tstd 1 [(Ts + 460) .. pstdJ Qw = Qs/ Xd Vmstd = Vm .. Y .. TSld .. (Pbm + L\H / 13.6) 1 [Pstd " (Tm + 460)] Vs = 85.49 .. 60 .. Cp" '~L\P"" [(Ts + 460) I (Ps eMs)] Vwc = Wtwc .. 0.04715 Xd = 1 -Bws APPENDIXB North Yellow Cake Scnlbber Preliminary Velocity Traverse and Smnpling Point Location Data Field Data Sheet YeHow Cake Dryer Baghouse Preliminary Velocity Traverse and Sampling Point Location Data Field Data B North Yellow Cal(e Dryer S!crubbe.r Prelim 8 pts blank Facility Denison Mines - Stack Identification North Yellow Cake Scrubber Date ~t ,S r-<t- r - Sa rometric Pl'essu rc PbmZ'I-[,'Q in Hg Pbp C ~'S'd in Hg N 0 Static Pressure (PcS="' ('::) t..{O in H2O B Estimated Moisture (8ws) 10 <x) Sample Height from Ground ~ 6 _ feet A Comments: -- Stack Din 18 Reference: 0 ------- Ports are 9.5' Upstream from next disturbance . - Ports are 9.5' Downstream from last disturbance - Traverse Percent Distance From: Ports Point Diameter ID Reference A B C D E F I 3.2 0.58 0.58 t,iO ; ()'-f D "'1'\ ,f)"/o <>fiJr HIO 2 10.5 1.89 1.89 .0"1 I) v\J"..('$' 3 19.4 3.49 3.49 "'Ill[ -6 Lt'j tdO ,o~~ 4 32.3 5.81 5.81 oi) ._ ·6<.iJ Ct1 • &,-0 !Of) , J :;-'S--1;-~¥ 5 67,7 12.19 12.19 6 80.6 14.51 14.51 f,'P . uv/() loP . ~ f)' 16.11 {Y~ 6'-'5 "l"i' 7 89.5 16.11 • <..('1.> ,/ 17Y " lfi5' til"" 8 96.8 17.42 17.42 . i.lS-' _. -- i Averages: Ts L Flow ---- I~P ~LlP -------- KEY=> f) / ') ~ Field Data Sheet Date: -[;/ Traverse I TitTle DGM ~ Clock Min (e) He; 1 &1 A1 0 1'15·~&\ 1 is "t>~ (p'ti 2 30 1. lJ '0 :J:f!? 2 45 '2---'1O ,4't't 3 60 ~~~'i;1\ 3 75 &'ltD· ~~~ 4 90 I~ 11. {; z,o 4 105 3'if\·11-'t 5 120 ':>1 r.·f~1 5 135 ,..?~~ . ttt -Vt 6 150 ~3j ,~z,&- 6 165 ~I{O. i ( J 7 180 ~l\q ·.J,n~ 7 195 i -;:;J'1·tt ~~ 8 210 ~f'.'6U\ 8 225 11:<; <1;1/ \,"·",1 240 ~<65:t~5 LiP LiH (inH,o} (initzO) Desired Actual ~646 .-'}t. .1.r't- ~o~ .i-~ .r+~ . Ot() , ~LA\ 'W'1 e'O'i~ ·11/ ·11/ -0t1~ ~ tt>t1 ,to '1 ·O~ .¥) ·St~ ,.o~$.{ .1-,} . -:t 1" -05b «:'-7 ~ 'o'''S -C~b .q(( .t1~ -o5'D -<6'1 .(¢~ ·(){S .)fO -~D ·Of.(~ -<£ D . S'D '04:)_ t\} '{\P ·DSV .<6\ ·~1 .()'i~ . kO .~b ;tl5D 1J\ ~~~ ,v! t/ (~4·Y) (._~_ -":7 Average -J Additional (Extra) Leak Check Inf / r \: 7-'( f:\\..U"- Vac ("Hg) DGM before Leak Check: ?~j" }75' tD~o -- TE'TCO Filte~~~ Sample Box._ft __ _ ('-~_\._----.--------- Operator: _---lL __ !--________ _ Vacuum Temperatures nO) (inHg) Stack (1,) Probe Probe Our Filter SfOuellt ~ lvO 1..-)0 ':z.l.e 6 ~(p~ {!i v( 1---'1 '1. [ .. ')0 1-,)5 2.->1 01-- 1, LOa 'tvi't 1,,(JU ~.(p "f., (e0 '1/ ~~ 'l-~f..(' 1",/\ 1,/f--\ It) v q~ '1.<vf t~vl t..-(1 ~& "> 1S'" -tC;5 .~ ~ '"' 1-5'Y _g--5L ~L C1S inlP 1\.\~ ~~O ~"1- 9 C1( 1L/'} 'J,v( -s zt;~ ,s~ \? Ci\ 'l.10 ~~V '" ('c ~'1.. [;; t10 17 .~"S 1. cJ'D ?5S C:'f (p /..1\ \ 1/J~ '19, 'i 1. c,f.t; S~ f" ct l \ 1;,cJ... J ~7/~:r ~y+:V 4 \ [9 ~1; 1.lt{'\ t\lO '1~ ~¥ lit; 1,0 ~~ z,~y ~'-\0 1~& ) !IJ~ •. ~ ?\C6 t7!2 r'l50 1/i#vl f.R ,.jj C(' '1 q~ ltl~ 'Z. ~5f rl .-z..\o (0 .t. I ,V"" ~ ------------------- Rate (fe/min) ~ , .r" \ ...... DGM After Leak Check b~\)\'J~ ?~S .0DO il I nGM Temp (T",) Out In 1t -:ry +& ~ ~ <6> /r~ q-O 13-~6 1-~ T'l 1 -; Page -1_of_L_ Run I sO N A Stack Diameter 18" Port Reference __ 0,0"_ Ports are Ports are ~ Upstream from next disturbance 9,5' Downstream from last disturbance Assumed Moisture -1/\' { Probe ~ 4-13 ~)o Cp 0,84 '1(", ~ '":fro ?J t -:j~ C(6 Nozzle Calibration b ~ '3;;.( '>*' ~YV Avg Dn • )..,$ ( inches ~f~r SZ' ~ Gas Bag H-c z: 1/ ---1-)( fLi--- "1-C1 ~0 ~ k1 Sf 0 b'vt ~() 9)C/, 9:J <;:'f '-) Vac ("Hg) 'L7 I Console 3 Y-Factor t · Db b L\H@ (, IP'i!in HzO Leak Check: ft;/min V:.1C in Hg Piter Rate [IlH~O Barometric Pressures z'-<. Cob inHg Hg ,, __ -'--_--'-____ in HP Pre -P f\ -"0\(-,' '''1-,. ~ ~T ---- "2..), D·D ,1. 'i ........... Water Collected Time Sampled { ()/l-y' R /il '€i f g ('\ 'Z-L[D 4 min , f "\ Review ctr l K @T" K= (C§Tnl Rate (fe/min) 0. DC) (0 VI q (t} '70 vl.,? /'" 5 li" ~o . /--.It? (p (,- "So "i? ~ .t; .,0 r.r.C: ./ ,fiA.?. ____ Fidd Data Sh~ct ."" I TLTCO 0· hller·~4 .Z"~._ Sample Box V ' Plant lknis Hl , 1ines \ \' Date-~ \ 1(.1"\, l.iL ~j Location: Notjrl\Ycllo\Vcakc Dryer Scrubber Opcral()r: =-p: /) rraVt~rse Point DUM II L\P I -.-JI-------r-'---"'-(I:', .. tlq«() i.~rnucl1tl In ~~o:L-J--~~~~~~L~JI 'ff 1,1(, IL~?::=JI[t ~ ~&<r~ 12~. {; I Zs~lif'lf{1lT? 255 1I .. ~ql{,·l.{~q ll ·o"f01 ·1( ./}\ I /1/ 1{6~ /..{(j (11 lhv ~'r <63 2 3 3 4 4 5 270 285 300 315 330 Bq7S-'f,lv'lP~.c; II~o ~oll511 tDO 11I..trr:J-~z»I~&II -Gj't1 t15 t:) -=-----l 375 6 7 7 8 8 390 405 420 435 II L.f,~_"I.lf"l;J -o~41-Y 0 I-~ q 1I(IJll ~"i:-l [>~I~:J&125iLL;[PJI ~il 1 01- I~:o~ I 480 II ~t.5'~4? Fl/\, tt tA.i ~1>r)( I 1 l,tt ·iZi Page ':k ui 1..-_ Run II I N BO A Slack I)iamekr _Il)' Port Rdcn.:nc<.: OJ)" Ports are Pori:; arc ~ Upstream from nexl dislud)ancc 9.5' Dowllstream from last disturbance i\~Sllmcd tvloistklp::\o Probe 1.. t N,O~.~pli~r~~\ 4-13 % CP~ ,rz,J't-. ~5t /\.V I [) 'I 1/ \ ,r'-. -- ._, g Il • 7~ 1 rnches \,,);; Bag \-\ L V CUl1Sl'ic"~ Y-iactor \. bO\{; "H~: , @ ,-.\p""'~\illll~O Baruilletric Pr-cssurcs 1'111--\,\00 in!!" III ~."""'._._ .• r ._ .. ,.-) .... _. t> Pl" /l"\'S in II" I\II'._~ ~_-Q~~.~: .. ::--in 11:0 Leal ("heck he i'l\nlin ~ .. 1~Q.hl I O,Vb '-f --- vac.IHIIg. ~ }'i PII(lfl{atc ~-t!J. D '" ~ .:Cs -:/ <-t?; /.1 Water Colb:lcd -:> . ..--(\.Y [! rime Sampled tiL0 ~1in Totar ~y-, r 0\1)~"'" -"l -t.,. ~-V . '6 I ! t" t;. l' ) ')('t.S ~#-~l( G~) V' ~ Rc\"ie\\ ;\\'~ragl! 1-~tt ~ 011 Q1·i ,j • "Ll0 ; ~ OJ, DGM before Leak Check Vac ("Hg) Rate (ft3/min) i I ,,~ •• /J 'OJ < v --- DGM After Leak Check Vac ("Hg) --~------ Rate (fe/min) K K (1.1':·j'1I1 iu~T!1; ~, tJ FieJd Data Sheet "1.. .,TETCO J\ Filter ~~) Sample Box_~_-1 __ _ ---- Plant: Deniso:q M inqs Date: < \ ... $'\ ,"1 J \ \. 4 v Location: NOli~1ellowcake Dryer Scrubber Operator: ttv'"'\ \ Traverse Point Time DGM L\P i.lH <;nH20) II Vacuum II Tel~peratures ;"1') DGtvl T~mp (Tm) crock I Min (8) ne, (ina!>, II Desired I Actual II (;nHg) II Stack(T,) I Probe I Probe O,;[ I Filter I Etl1uentll Out In 1 1 I~-;.~ I 0 II S1{f-S't> 1-IL-o-9flr-·-~ \ I -Ci.\ II ~ II lLD '-2-,4:1 ~~'iL-r{~ \ II f? I "1--) 15 n57 ~. v11S~ . tlliQll~'1Y -T·~f)r II 'Ull db 11/ ,q 11.7'>12:(; I S--YliYrl <l)~- 2 2 3 3 75 115T5'1t1'11I~()"f?1f\'1) 1 \,\ 7 1~a,-1I~1X' "I t-', 01 r'?~1~5L;t 1:7(;; II <; 'l---I '7; Ct. 4 90 H:;-~~-70D II ·o1'S 1I1,1tY -n,'1D r q:ll I'ZO I~Z v/11/-u~i'-t~ 1 ~~Iv? I l6-"'F 4 105 II~S. ;~'1l~II (·l)m! [.(") IU~[J1mYr'l~1 1wTT I It..:GI~:r II ~~ I ~ ~ 5 120 II ft;()~.I~<71I ·OY()1I r,'t~ml \·~'111 (tJ ~1 (1 \ 11AQ 11.(;L-lz Cl{ l6{oj II~) 1 'fr& ~ 135 II (/t~. :75"'(' II 'b~IIt'1~ 1f.-;YJLv II fl u f~'-'t«1 Z;~I z»)Js-D -II ~) I yS( Q ~~I --~~~~~~~~~~~~~~~ 6 &~~ 7 8 - 8 '----jl I 210 l~rn{l~ \,~ L~--r'tJ f~ I G""ltml ~'il ~~ 225 II (1/;/ .u.1.,~..1-'-&01\·t,~ [~-I i{~~~·(P"L~Cj2p.:o;=-~»)(: q') 195 11/; ~'o ·ll&:nl-o'1"5r~21l \. Lnl r l~3-1 '0)~ I .~~s-: I L5~ I S-r-II ~<C 11 V tr,~lP 1 240 II &Zj ";. )O{ 11 ,,-----lrc I' 'II ' "---U \ \ T= 'rotal I (g&,~07 ,/ ~ ---y -dj ~ t --Page __ .Lor &_ Run # ""l/ r aO N A Stack Diameter J 8" __ _ Port Reference _0.0"_ Ports are 9.5' Upstream from next disturbance Ports are 9.5' DOVv'nstream from last disturbance Assumed Moisture ( 4-13 qu Probe ~ -} It;? Cp 0.84 Nozzle Calibration .)&-\ 3\s'\ ~5I"t-'SyG---1-"'---- Avg Dn • 3~ '? inches Gas Bag I'; C ? Console~ V-Factor I ~ C) 1} L9 . I I c.\H@ l' V-1 1 in H20 Barometric Pressures Pbrn _ '1 V{. )'D in Hg I A Pbl' z ...... t ...... ( ~ __ in Hg Pc; --O . 0 L{~ in H20 Leak Check: Pre Post ft'fn1ll1 O· () b~ """"7 vac inHg 'L?,. ~ PitotRate2 in H20 ,Oz..s:' -LJ7 ~ /7 01 .-. Water Collected 0 t !' L g Time Sampled * 4 () ....;2f '-1. Y () min Review \ ~\ -\CZ--~\ Average 't;' 0", ~'-b "Ad .~iJ~~~~\) V\\.\~\.>k)~ ,; e4 ~\(l;./L-() I/,g ,r,J.::lr' r ~ .~\'6"-'·-1 I K:::: i'JJJTm K= @Tm . ----_ ... -----,,-------I ---_ ... --_. ----. DGM before Leak Check Vac ("Hg) Rate (fe/min) DGM After Leak Check Vac ("Hg) Rate (fe/min) (p~).?O) r 0 ,00 (y (pq~t4 D'Z/ t1'-O· a~ '6 '0 I I I \ ~'\c; herd Data Shed .. J TI·:TCO rx hiler .5:~..\ Sample BOx_._._ .. V_.: __ _ t.f IS" <?,O <is- C; ,( ';0 V'.( & It{ )0 If 1 f( -;0 q(" ~ Plan!' ----.-7""\---+ Location: North 'f1lo\Vcake Dryer Scrubber Date:' Operatur: II' DCj M (n'. rr"H,crsc Poinl I ;\11 iI:OJ Desired I Actual (",lip II Stack (T,,) I Probe I Pr(>(,"Oul I Filter I Et"Illlcntl! Out III ,\H (InH . .o1 II V"~""1Il 11 Tell~pera!lIn;s ~,------11 f)(ii\IT:"II>(T",) L\P {CY.'I 240 1/ lt41.~o'Vllos5 II . t'~lFSf~ 111-II !! 1/ 11&~' 11-}o 107D I [,I.P II?; -:} I <:rr 255 111o)R'lJL,_{j~t:)JI-,~J I 91 l' IL.1-ILJJ L I Z 5"") 11 3\ I ~ ~ y I §\-L I~Jl <10 2 ~ ~I I ~i~-!fiJt}~ ~JI : ~~~JI \C,~~w-II ;;; Ih!~l~.-.y-t-+-:;;;;----:--t-t---;:~~ ~ 300 U'"t71-t&)~r-OJ9111 'll -rT:·~r-lr--~lrt~~\~-Iz.-~--:ST2.II-oTz&-3~rZ?TII yC; I ~1 3 315 11_1:r'?~'~1)II IO~~JL-t"J I (. t 1 11 L/ II I lQ-10-'> 61 zCJ V I 'z,l9Sj' 1 ~. -b II 5f 7l q 0 i 330 II ~~.' 1'1) If ', () ~j I~ t, "'7YT\~~(:rIl----q II t~~lt '7 D I .~\.\~ 1 ~ S\TU'\il t6sT~ q 4 q ( 345 II ~1R, 7'[»t?J~[ \ . ~ t l· ~ S1r-~=m_1 ! I 't &Vl l -z {g 1'~~ ~~ I et ~ Il5L<i I 10 360 IIl·Tt.~br-l~ ,t)hblf-lt~ l (·tPt I~lf H<J 1 1i)~1 ?_(;~1 2,c,,1 5~ I[~fp l q, l 5 ~rl ---r--~~~~~~~r~~~rl 6 6 7 7 8 tr~ \ Il i~'·q\ Total /\\'crag..e 405 II 9 H. ')~'111 ·dPDJ/ ·Cjl-I-"'-~1115 ff -H~rtG~1 Z(p~lri~;t-l f.J L II -Jrtl 1-& ~l ,q;~~,·~~l~.)(.\ J\<r J 1m i~ 435 1~S17l/l~IrJQ?( :s r; ml-'-l-"-,&~,?".---f-''''''-+-'''--l------;;--,=~~r+--:---'--l 450 II~I{"~ ·1?-P11~~! j,,[1) [ \·1/91l7lrJ], f I ~7'\[j~(g \ I tCd [l;() II c;;~ im>{V ~1<67V\'~'~~ If;'ok b 11-~1-1 . s1i~1 i{'\ '-+1{eD If! ~ \ j'1-let-I (J 0 11'60(.1 I s;-~ 4801 tA v'{. 73 :r I}-Uf/5 1 l,le . ~ o-s IL-JI I--Il--il ---11 ~' c:ts i~.{;--~ <6 ' V l' ~ 'L; ,i . «~q~-:.~\~ -; .... :-~.-!---.. - ------ L' 1-:t~J;' , 10. ( l -\ \,.; '~7r~1 1\ cg ,G -----l a:;<-{ ~ 1 ~s·~ ~---~ .. ~.---+ I'ag~. ~ 01: /'L-/ I{un ll V_. r BO N A Stackl)ial11et~r Ig" Pmt l~d\:rell(l.; .. 00" Ports arc 9.5' Up~trealn from nexl disturbance Ports ,lre 9.5' !)\)WnstrCilm i'rom last disturl)<lncc /\sSUll1cd M()i~tlln; 4-13 1\0 Probc Z1k Cp 0.84 Nlln.k Ca libratioll ~ . »1 . )~-t-<5S"'t Avg fJ" • '3ff <) inches Gas Bag 8L'" Console ~ Y-Factor-I·-b;-t? ,\H@ l-lo~ \ ill liP Ll!~,.k Ch(..~;,.:J...: n""tIllil vat: il~ Il~ Plhll Riilc 1011,0 13aroll1c!rtc l)r'csslIn:s Ph". .'2, , .. t · SO . . ill [ [~ I'hl,_ z'-'L.~!:L,}.-in Ilg I'" -=-... Q_~_.Q .. ~.~ ___ .. _ in 11:0 o ~)I~O ~ 6~E65" '2-. '7 lrg' 0· 0 .62.-'),..- O,D /) ~--?: tfr) D ... Z--s. Watcr L'olb:k:d ~ Z ~< '( . .. . /' ,. IIIlK :)alllplcd :0{ i " u b [{evil'\\' K K -t-L min th {d'T'i! (11:'1'", DGM before Leak Check Vac ("Hg) Rate (fe/min) DGM After Leak Check I Vac ("Hg) Rate (fe/min) .\.-~ r;)t>u.J~ ( \ I ~ " ~ _" \ . , I S \J:;)11 \ \ ~\ Ov \ n\! \j \. S -V, Yellow Cake Dryer Bagh10use Prelim 6 pts blank Facility Denison Mi nes Stack Identification North YeJlow Cake Dryer Baghouse Date 5/{ )" 11'7.- r Ba It"ometrk Pressu rc B Pbm 24.<00 in Hg Pbp~1, o~3 in Jig -0 N Static Pressure (Pn) ...... (. ( in H~O ----- A Estimated Moisture (Bws) J % Sample Height from Ground 10 feet Comments: Stack Dia. 16 Reference: 0 Port~ are 57" Upstream from next distllrbance Pons arc 468" Downstream from last disturbance Traverse Percent Distance From: Ports i Point Diameter ID Reference A B C I ]) I E I F i 1 4.4 0.70 0.70 ,')\ ,ft{ .J~ ~3 2 14.6 2.34 2.34 t'Y-> <1'( vt\b C{{ 3 29.6 4.74 4.74 llO (0 \ t~(" (1;( 4 70.4 11.26 11 .26 l'l..6 ,.,'Z_ \'1,;-( qv 5 85.4 13.66 13.66 ~i.£ lOt. I,~?-<t,q-. 6 95.6 15.30 15.30 .1,..~-Iqt. U)'t." tqlt -- Averages: Tg L Flow ---- ~p---- KEY => _I 2JiJ(/ __ Field Data Sheet D Plant: Denison Mines Date: 5 ({ 5" ( \?,... Tra-vcrse Time I DGM Point Clock Min (6) . (A\ 1 10 :r;r 0 rz.I.z...,,'l 2 to 1,,'L i:\ ~C 3 2.0 t~g'<H) 4 3rv 1~{~1. !)O 5 t(.0 15S,BSo 6 50 ibc..t,o"lC H'.2..\ c,<> nLn1 ~ 7 if) ISo. 1.~)" So l88,.,0.( L1't) ICf(",z'iO tDO 'Lot.{.o'h"'- do Z i t·'100 rz.:zt nO Z/C={.510 Tota! a~ . d ,tu,1..l{\ Average Commenfs: Time Baghouse ,iP ty,~o [t1~" \O·.~~ I V>\ IVI(O/ I 1'0 , I \\',0"') I lJy TETCO Filter >G:n... Sample Box B ------------- I ("~:») ~H (inH,O) Vacuum Desired Actual (inH~) ;3fe 2.o<{ "2.o'{ n "1, ,'}"" 1.'0'4 'l,t)'\. '1 ~ :'5 \.'1.) t.'!{ n ""i. ,~-.(' t,~ -r \I~)~~ Ll ~ 3'2.-,. \,'S VIS :) \)1-t,)~ r.l'g :"~ ., \ 1'11. I·'l :> l'5u I ,~~ {.(,,(" :3 1:)0 i.",<., L(.(i:; :s .1..& lJ8 t,{S 3 ,z~ l.iB L:re ::s ,'1. '1' i."}2 .. L{z, '1 '>/ (p·lytt1 ,/ '2), ?, -{ 01 ~{e ~ 1 -,J • J {." \,11\ Time Baghouse ,iP H',~{ ji\:; tl:1{5 l{(& \"L1•OO q~ \1;, i{ I 5,\ Location: North Yellowcake Dryer Baghouse Operator: K \c ~ J,A-1 ¥l~Gr- Temperatures (I') II DGM Temp (Tn,) I Stack (T,) '1<S 0: ,r' P iq ( 110 'i1-qs 'f'? 9q lot go t t<O'Z,..- tot. 101..- H'e>{,/ / Cfb,l"l Probe I l'robcOul I Filter I Effiuent!l Out ?SO ZbO 2"0 ~1' -~{ l 7..<j"f' LCcr-z{, ':}-5r 7~ 1,(rt. '-~t 'H. ( LI 80 '1){ '2100 1.(,0 k'l B~{ Z1Q '2.<.,( 2(",( S'R gf "00 ZiP ! ('f8 L-SJ~ Ss ~1- t'-{ ... ~ Zf-r 'Z1) S(g ?>3 7.).;< 2ft, 2.:f~ :H 5" l'{,"\ (( .. <.{ l.(,~ Sz... 81- 'Z<i5 2C:;" u,\o 5t{ 81 2..)4 LII>3 '--(,3 55 &=t l..a...JO 1..""1 V .. 'f-5'1--'to I In {,~ ~'1 ""LC 7J ~Zz. 1'-i '-7U . \ "'15 I) If {fa -1'1 t~9~/ 16S H~r~\s v->e\!-?C£~ DIjLIIi.~y kst: Page ~ot~ Run # ___ _ i B AD N Stack Diameter l6" Port Retercnce __ 0,0" Ports are Ports are - . 57" Upstream from next disturbance 468" Downstream from last disturbance Assumed Moisture ~1, Probe tS -(? Cp 0.84 Nozzle Calibration ; 2'76 I Z. '1h I z7b ,Z7\:, ------- AvgDn 'Z'1,b inches Gas Bag Amhient Air Console ~ Y-Factor ~ ~cO-z, ilH@ }\,% in H10 Barometric Pressures Pblll "Z 4~(""O inHg Pbl' '2...\..t<S'3 inHg Po ; Z{ in H20 Leak Check' Pre Post tt'/min 0, eo:t ~o8 vac in Hg. ZJ·O ~ Pitot Rate Q ,'0 ~ rnH:O 7,'0 'tl ·O Water Collected Time Sampled j q .() g b .,.jf 11--0 min Review fJIJJJ.. K~ @Tm K= @T", North Yellow Cake Scrubber Satnple Recovery Gas Analysis Data (ORSAT) Yellow Cake Dryer Baghouse Sample Recovery Gas Analysis Data (Ambient) Chain of Custody Lab Analysis APPENDIXC c North Yellow Cake Dryer Scrubber METHODS Facility: Denison Mine Stack Identif1cation: _N_Y_C_S_c_n_lb_h_er ____________ _ lMPINGERS IMPINGERS S~33 Sq~ It IMPJNGERS IMPJNGERS Final (g) Initial (g) Net (g) Final (g) Initial (g) Net (g) Run: drop Ollt c.,j~fl 5~ /1 ') t ~ti • ,~- Run: drop Ollt ?&U D (PG.l.{.~ /75-''1 Run: ....L drop out ----Sample Box: ---- Impinger Number 2 Ill...i.I.lJ Initial Volume of liquid (H20) in impingcrs, (mJ) I 100 I 100 I Silica]cl] -Zl)i4 "'lLL ,){1~d" (p r~( ~ q 2.0 If sse .5 ~ 3'2,( S,B( ( ~o8,3 eb).~ (17i~ 3q It ~{t{ S'd 5"-:7. ( Total (g) ======== ----Sample'Box: ---- I Impinger Num6er 1J...llli Initial Volume ofliquid (1-120) in impingers, (m1) I 100 I 100 I Silica Gel S}~l to';-, &: S-1&--.() Cttr. ~ 0., r{. . () S'10(( ~"~1,~ .s-efa d/ ~o815 85<f,8 ZfJ 5',.1 f 'f -:··f' t 1. '7 ·~.o SV ~L- Total (g) ~ 1 __ q. 1/ ======= ----Sample Box: ---- hnpinger Nun15er -1-I L I .J,... I 5 Initial Volume ofliquid (H20) in impingers, (m!) I 100 I 100 I SiIicaGel Final (g) ..,.-----+----+----+-----4-----+---- Initial (g) CD "4. ~) -------+-------+-------+-------r------~-------Net (g) =================;========================= Total (g) ======= Run: ----Sample Box: I 3 I -L I 2 .. Initial Volume of liquid (H20) in impingers, (rnl) drop out I 100 ! 100 I Silica Gel Final (g) I Intii~~)=======:=======:======:=======:======:======~ Net (g) . ==============~======~==================== Total (g) ======== 01' /1'I.--7~ P1ant. __________________ _ Location ( r"~~ Analytical Method_~_)+---------- Date sf £</I? Test No. -~I~+-. /-"" """'"'/' f Gas Bag No. . '\ v ,_ Ambient Temp_~fi~--=O;..... _ Operator -~t ... ~:P',c~,,\\-\- ! f Date $f-(b l rt Test No. "J-. Gas Bag No. Id:L ~3 Amoient Temp ~ Operator Date -----Test No. ____ _ Gas Bag No. ____ _ Ambient Temp Operator ____ _ Gas Actual GIIS RelHling L{-3 '-(-~ ~-~ f~-S-\'1. ).- Gas 2 (Net is Actual O2 70 2 was determined using a gas analyzer CO is not measured, as it has the same molecular weight as N2 Net Ncr 1..{-5 "-( '-> '-f-)' lC\ '5'--L)'Z Net Average Net Volume Average Net VolulUC ~·5 ! .5-, Avcnlgc Net Volume Yellow Cake Dl"yer Baghouse Method 5 Facility: Denison Mine Dat.e: ----------------Stack Identification: _N_Y_C;.....;;..B....lag ..... h-.;.o...;...us~e_. _____________ _ IMPINGERS Filter Number IMPiNGERS Filter Number IMPINGERS Filter Number Final (g) Initial (g) Net (g) Final (g) Run: __ \___ Sample Box: __ G_. __ Impinger Number 2 e=--t I ~ I ~ I 5 6 Initial Volume ofliquid (H20) in impingers, (ml) ]00 ] 00 I I Silica Gel I Go9.0 ~"'Ll .t{ S<t),~ Cf ~.C;.~ ~ l,Z(IC-G,/ @( ~ 68 9 .6 Cfl41D ... ItP ."t., 8 .t{ ~-'O ~z. t.~ Total (g) ======:::::= Run: ----Sample Box: ---- Impinger Nunlber .. .Llhl LI~ Initial Volume ofliquid (H20) in impingers, (m!) 100 100 I I Silica Gel I Initial (g) ------~~----~~----~r-----~~-----~~-----Net (g) =======±======±=============~======~====== Total (g) ======== Sample Box: ------~======~lr,-n-p~in-g-·e-r~N~u-m-¥5-e-r--~--~~~::,-----. Run: ....t.12-1.4..-11 L Initial Volume of liquid (H20) in impingers, (ml) 100 100 I I Silica Gel I Final (g) ___ --II--__ --II--__ ---II---__ --II--___ ~I__--- Initial (g) ___ ~I--_---II------II------II-----_I~--- Net (g) ======~====~========~====~======~====== Total (g) ======= IMPINGERS Run: ____ Sample Box: ___ _ Filter Number lmplnger Num6er Initial Volume of liquid (H20) in impingers, (mt) 100 100 I I Silica Gel I Final (g) I fuili~(~=======:=======:=======:=======:=======:=.======= Net (g) _ ====================~====================== Total (g) ================ ~\ ~ >,~ ~~:~':::~~~:"1~7 ?j~:~:}~~~;," ~~rl1~Ji~~~ :l')/~~~:~~~{ ~~.:~tt/~ Chain of Custody Record TAL-4124 (lOO7) Client Tetco • Temperature on Receipt __ _ rica Drinking Water? Yes 0 No 0 THE LEADER IN ENVIRONMENlAL TESTING CbailJ.of.Cu.sliJdv Number Address' .. "C~.::::·:·"·:::::·.::"":".:":":·"::-:::::.~;;"·· --.-r'.-.--.. _ .... __ . , ... ______ , .. _ ... _ .. ~_. 391 East 620 South ..... '801::492-:9106 page_L of City r·····~· ........... . ........... .: r State IZlPCQo.e.. . ...... Site cC;;:la~ Lab Contacr Ana.lysis (Attach Jist If . American Fork Ut .1,&,4.003 . ScottChrlstensen,DarrlnPalmer morespacsisneeded) Pro;fJt;i Name and LcC'alicfI (State) Denison Mine~q12 2nd Q.ll(:lr~er Contract/Purcha.se Order/Quote No. Canier/Waybl7! MHui:Jer Matrix Containers &. Preservatilfes 0 Sampfe I.D. No. and Descrtptkm D te ~ ~ 8 _ a ~i§ (Containers tor each sampl~ may Dr) combiflf!Jd Orr one/too) a. t!. _! ~ l--'~-+-'~-=~+--+'-~"""~"'h ~I ~~~ ~. ~; & ~' .L,.~ . 5932 Rl filter and beaker • ·1 ' X.' X_ , 5930, 5931 Rl NYC filters and beaker J ;!] Xii X i1iX'rx 'I 5933,5934 R2 NYC filters and beaker f ..l i J. )(1 X Ix: X ! SpeciallnstruotionS! Conditions of Reoeipt -~~---t-'-I I ' i +-.... l ..... _.I·_ .. ·+--+--tl-r I , I I t I .-Lt.J-t-+--+-I I-+---+1 1 __ i I I ~~~ __ --------L_--'-----'-~~..L..-.....L-",-------"""''-----J.....-'" ~rD_._.J---1_-L-1- Possible Hazard Id$l1iiflCation Sample Disposal " fA fee may be a&e$Scd if $M?pf~$ are retained o Non-Hazard 0 Flammable 0 Skin Irritant 0 Poison [J 0 Unknown 0 Retum To Client 6 Disposaf By Lab 0 Archive For ___ Months longsf tha.rt 1 montl'l) ac, Raquiiiiinents{SpectiY) o 7 Days 0 14 Days 0 21 Oaye 0 other as Det method !~; { 1-I .• ~1i.'1)e .: Db 7. Rscelv9d 8y I Dele I Time ~~L .;; V --~r5;,,"~!L-.!.l.f 2 """,Iv.., By ""'''' .... 1 =fim_O __ _ 13. RclinQtJished 8y I oare I Time 3. Aeosived By I Date I TIme Comments When Complete Email to:DeanorPaultetco@tetco-ut.com iiiSTRfBUTJON: WHITe -Re!urned to Client wllh Report; CANARY -6't8ys with the Semple; PfNf, -,ISIS/a Copy SDC No. Order No. , ~.~ ,~ ~ .'~ 45037 TestAmerica rptSTLRcbTitlc vJ.73 TestAmeric:a Laboratories, Inc. Analytical Data Package Prepared For Denison Mines (USA) Corpo Denison Mine 2012 2nd Quarter Radiochemicltl Analysis By TestAmerica 2800 G.W. Way, Richland Wa, 99354, (509)-375-3131. Assigned Laboratory Code: Data Package Contains 19 Pages Report No.: 52118 Results ill tbis report relate only to tbe sample(s) analyzed. Client Sample ID (List Order) Lot-Sa No. Work Order Report OB 10 ----' ...... _........ .. '-'--'---' --.~~---_._--,-" . 5930, 5931 R1 NYC filters J2E21 0429~2 MTNPH1AD 9MTNPH10 and 5930,5931 R1 NYC filters J2E210429-2 MTNPH1AC 9MTNPH10 and 5930, 5931 R1 NYC filters J2E210429-2 MTNPH1AA 9MTNPH10 and 5930, 5931 R1 NYC filters J2E21 0429~2 MTNPHiAE 9MTNPH10 and 5932R1 8aghouse filter J2E21 0429~1 MTNPG1AD 9MTNPG10 and be 5932 R1 8aghouse filter J2E210429-1 MTNPG1AC 9MTNPG10 and be 5932 R1 Baghouse filter J2E21 0429-1 MTNPG1AA 9MTNPG10 and be 5932 R1 Baghouse filter J2E210429-1 MTNPG1AE 9MTNPG10 and be ~ 5933, 5934 R2 NYC filters J2E210429-3 MTNPJ1AD 9MTNPJ'10 and 5933, 5934 R2 NYC filters J2E210429-3 MTNPJ1AC 9MTNPJ10 and 5933, 5934 R2 NYC filters J2E210429·3 MTNPJ1AA 9MTNPJ10 and 5933, 5934 R2 NYC filters J2E210429-3 MTNPJ1AE 9MTNPJ10 and (3atd, No. 2144068 2144069 2144070 2144071 2144068 2144069 21440'10 2144071 2144068 2144069 2144070 2144071 tHE L.El\bER IN ENVIRONM£Nl Al TESrlNG Certificate of Analysis June 25,2012 Denison Mines (USA) Corp 1050 17th Street, Suite 950 Denver, CO 80265 Attention: Dean Kitchen Date Received at Lab Project Name Sample Type SDG Number I. Introduction May 21, 2012 Denison Mine 20 J 14th Quarter Three (3) Stack Fi1ter Samples 45037 CASE NARRATIVE On May 21, 20 12, three stack filter samples were received at TestAmerica's Richland laboratory for radiochemical analysis. Upon receipt, the samples were assigned the TestAmerica identification numbers a<; described on the cover page of the Analytical Data Package report form. The samples were assigned to Lot Numbers .I2E21 0429. H. Saanple Receipt The samples were received in good condition and no anomalies were noted during check-in. HI. Analytical Results/Methodology The analytical results for this repOli are presented by laboratory sample ID. Each set of data includes sample identification information; analytical results and the appropriate associated statistical uncertainties. The analysis requested was: TestAmerica Laboratories, Inc. Alpha Spectroscopy Thorium-228, -230, -232 by method RL-ALP-OO I Uranium-234, -235, -238 by method RL-ALP-004 Gamma Spectroscopy Pb-210 by method RL-GA-OO t Alpha Scintillation Radium-226 by method RL-RA-OO I 2 Denison Mines (USA) Corp June25,2012 IV. Quality Control The analytical result for each analysis performed includes a minimum of one laboratory control sample (LCS), and one reagent blank sample analysis. Any exceptions have been noted in the "Cotnillents" section. V. Comments Alpha SpectroscollY Thorium-228. 230. 232 The blank activity ofTh-230 exceeds the detection Hmit~ however, it is less than the activity in the samples. The achieved MDA of the samples exceeds the detection limit due to insufficient saITlple volume. However, in most cases, the activity oftlle samples exceeds the MDA and detection limit. The data is reported. Except as noted, the LCS, batch blank and sample results are within acceptance limits. Uranium-234. 235. 238 The achieved MDA of the batch exceeds the detection limit from reduced aliquot sizes taken due to historical process knowledge. The sample activity exceeds the MDA and detection limit for the sarnples. Data is accepted. Except as noted, the LCS, batch blank, sample and sample duplicate results are within acceptance limits. Gamma Spectj'oscoPY Pb-210 The achieved MDA of the samples exceeds the detection limit due insufficient sample volume. The LCS recovery yield is just above acceptance limits. A recount did not improve the recovery. There is no sample volume remaining for fe-analysis. Data is repolied. Except as noted, the LCS, batch blank, sample and sample duplicate results are within acceptance limits. Alpha Scintillation Radi llm-226 The achieved MDA of the samples exceeds the detection limit due insufficient sample volume. Sample activity exceeds MDA and detection limit for all of the samples. Data is accepted. Except as noted, the LCS. batch blank and sample results are within acceptance limits. I certify that this Certificate of Analysis is in compl iance with the SOW and/or N ELAC, both technically and for completeness, for other than the conditions detailed above. The Laboratory Manager or a designee, as veritied by the following signature has authorized release of the data contained in this hard copy data package. Reviewed and approved: Erika Jordan [~w.~ nX\{)~) 2012.06.25 7-16:13:45 -07'00' Erika Jordan Customer Service Manager TcstAmerica Laborat{)rics, Inc. 3 Drinking Water Method Cross References " .... . "· .. ,r ... , .......... , ; DRINKING WATER ASTM METHOD CROSS REFERENCES __ J Referenced Method lsotope(s) TestAmerica Richland's SOP No. EPA 901.1 Cs-134,1-131 RL-GAM-001 EPA 900.0 Alpha & Beta RL-GPC-001 EPA 00-02 Gross Alpha (Coprecipitation) RL~GPC-002 EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002 EPA 903.1 Ra-226 RL-RA-001 EPA 904.0 Ra~228 RL-RA-001 EPA 905.0 Sr-89/90 RL-GPC-003 ASTM 05174 Uranium RL-KPA-003 EPA 906.0 Tritium RL-LSC-005 '.-, ," '. .. .".' .",.¥."" •• ·M .•. ,· .•...................... d '.· . ..•.... ............ . .... "'.,.' ....... ". " . Results in this report relate only to the sample(s) analyzed. Uncertainty Estimation TcstAmerica Richland has adopted the internationally accepted approach to estimating uncertainties described in «NISTTcchnical Note 1297, 1994 Edition". The approach, "Law of Propagation of Errors", involves the identil'ication ofal! variables in an analytical method which are llsed to derive a resLlIt. These variables are related to the analytical result (R) by some functional relationship, R =-= constants * f{x,y,z, ... ). The components (x,y.z) are evaluated to detennine their contribution to the overall rncthod ullcel1ainty. The individual component uncertainties (Ui) are then combined using a statistical modellhat provides the most probable overall uncertainty value. All component uncertainties are categorized as type A, evaluated by statisticaJ methods, or type B, evaluated by other means. Uncertainties not included in the components, such as sample homogeneity, are combined with the component uncertainty as the square I"()ot . of the sum-of .. the-squares of the individual uncertainties. 'fhc uncertainty associated with the derived result is the combined uncertainty (ue) multiplied by the coverage factor (1 ,2, or 3). When three or more sample replicates are used to derive the analytical result, the type A uncertainty is the standard deviation of the mean value (Sl?n), where S is the standard deviation of the derived results. The type B uncertainties are al l other random or non-random components that are not included in the standard deviation. The derivatlon of the general 11 Law of Propagation of Errors" equations and specil1c example are available on -~ " -~''''--'----.-------.----.----~--.. --.--.~-.. -.. --.-.----... ----.---.. --.-------~-.--.--------------.----'--.. -....... ---.----.-... --.-,-~ .. ~----.--¥.-.... -.. ---~." .. -.-.. --.----. T estAmerica rptGt~lIeraflnfo v3.72 TestAmerica Laboratories, Inc. 4 Bias COCNo Count Ern>r (#s) 'rota) Uuccrt (#s) lie _ Combined Uncertail1(V. (#s), Coverage F1\ctor CRDL CRL) Lc Lot-Sample No MOqMDA Primary Detector Ratio U-234/tf-238 R'itlMDC RstrrotlJcert RepOI't DB No RER SDC Sum Rpt Alphn Spec Rst(s) Work Order Yield TestAmerica rptGenerallnfo v3.72 TestAmcrica LaboratoIies, Inc. .. ___ ._._ ... ____ .... _ .... _B~port Def!!:~.itio ~ _________ . ____ ..... __ ... ______ ._._ ... _ ...... _ .. _ .... __ .. _ .. ______ ._'"_ .. An agreed upon activity level used (0 trigger some action \-"hen the final result is greater than or equal to the Action I Level. Often the Action Level is re lated to the Decision Limit. I The QC preparation batch number that relates labortltory samples to QC samples that were prepared and analyzed I,; together. Del1ned by the equation (ResultlExpected)-1 as defined by ANS[ N 13.30. Chain of Custody Number assigned by the Client or 'festAmerica. Poisson counting statistics of the gross sample <:ount and background. The uncertainty is absolute and in the same units flS the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background. All known unceltainties associated with the preparation and analysis of the sample are propagated to give a measure of the uncertainty associated with the result. lie the comhined uncertainty. The uncertainty is absolute and in the same units as the result. The coverage t11ctor defines the width of the confidence interval. I, 2 or 3 standard deviations. Contractual Required Detection Limit as defined in the Client's Statement Of Work or TestAmeriea "default" nominal detectioll limit. Often referred to the repotiing level (RL) D(:cision Level based on instrument background 01' blank, adjusted by the Efficiency, Chemical Yield, and Volume associated with the sample. The Type I error probability is approximately 5%. Lc=( 1,645 * Sqrt(2*(BkgJ11dCnt/BkgnldCntMin)/SCnlMin» * (CoIlvFctl(EfJ:)(.Ylcl*Abn*Vol) :;: [ngrFct). For LSC Illcthods the batch blank is used (lS a measnre ofthe background variability. Lc cannot be calculated when the background count is zero. The number assigned by the LlMS software to track samples received on the same day f()r a given clien!. The sample number is a sequential number assigned to each sample in the Lot. Detection Level based 011 instrument backgrollnd or blank, adjusted by the Efficiency, Chemical Yield, and Volume with a Type I and II error probability of approximately 5%. MOC = (4.65 * Sqrl«BkgmdCntlBkgrndCntMin)/SCntMin) + 2.71 /SCntMin) * (Col1vFct!(Eff* Yld "Abn * Vol) * IngrFct). For LSC methods the batch blank is used as a measure of the background variability. The instmment identifier associated with the analysis of the sample aliquot. The U~234 result divided by the U-238 result. 'The U-234/LJ-238 ratio fi1r natural uranium in N Is'r SRM 4321 Cis 1.038. Ratio of the Result to the MOe. A value greater than I may indicate activity above background at a hig)l level or confidence. Caution should be used when applying this factor and it should be used in concert With the quali IIcfs associated with the result. Ratio of the Result to the Total Uncertainty. lfihe uncertainty has a coverage factor 01'2 u value greater than I may indicate activity ahove background at approximately the 95% level of con fidence assuming, a two-sided contidencc interval. Caution should be used when applying this factor and it should be used in conceit with the qualifiers associated with the result. Sample ldentllier used by the repOli system. The numher is based upon the first five digits oflhe Work O .. dc," Number. The equation Replicate Error Ratio = (S-D)/[sqrt(TPUs2 + TPu(fn as defined by lCPT BOA where S is the original sample result, D is the result of the duplicate, TPUs is the total uncertainty of the original smnpk and TPUd is the total ul1ccliainty ofthe duplicate sample. Sample Delivery Group Number assigned by (he Client or assigned by TestAmcrica upon sample receipt. The sum of the rcpolted alpha spec results for tests derived ii'om the same sample excluding duplicate result whet"! the results are in the same units. 5 Sample Results Summary Date: 25-Jun-12 TestAmeric::l Ordered by Method, Batch No., Client Sample ID. Report No. : 52118 SDG No: 45037 Client Id Tracer Batch Work Order Parameter Result +-Uncertainty ( 25) Qual Units Yield MOL CRDL RER2 2144070 RICHRC5011 593.0, 5931 R1 NYC filters and MTNPH1AA TH~228 3.25E-08 +-3.8E-08 U UCIISA 66% 5.19E-08 3.00E-15 TH-230 9.36E-07 +-2.7E-07 UClfSA 66% 5.90E-08 3.00E-15 TH-232 1.04E-08 +-2.1 E-08 U UCI/SA 66% 5.00E-08 3.00E-15 5932 R1 Baghouse filter and be MTNPG1AA TH-228 4.65E-08 +-5.6E-08 U UCI/SA 52% 8.64E-08 3.00E-15 TH-230 2.55E-05 +-5.3E-06 UCI/SA 52'% 6.32E-08 300E-15 TH-232 3.43E-07 +-1.5E-07 UCI/SA 52% 6.32E-08 3.00E-15 5933, 5934 R2 NYC filters and MTNPJ1AA TH-228 8.57E-08 +-5.5E-08 UCI/SA 90% 3.61E-08 3.00E-'15 TH-230 1.86E-05 +-3.4E-06 UCIISA 90% 3.49E-08 3.00E-15 TH~232 5.98E-08 +-4.4E-08 UCIISA 90% 3.49E-08 3.00E-15 2144071 FFSR 5930,5931 R1 NYC fitters and MTNPH1AE U-234 3.61E-02 +-8.6E-03 UCI/SA 39% 1.34E-04 9.00E-15 U-235 1.42E-03 +-5.3E-04 UCI/SA 39% 1.25E-04 9.00E-15 U-238 3.34E-02 +-8.0E-03 UCI/SA 39% 1.34E-04 9.00E-'15 5932 R1 Baghouse filter and be MTNPG1AE U-234 3.44E-03 +-7.7E-04 UCI/SA 92°/\J 5.70E-05 9.00E-15 U-235 1.1 8E-04 +-8.2E-05 UCI/SA 92% 5.31 E-05 9.00E-15 U-238 2>.31 E-03 +~ 7.4E-04 UCIJSA 92% 5.70E-05 9.00E-15 5933, 5934 R2 NYC filters and MTNPJ1AE U-234 4.15E-02 +-8.1 E-03 UClfSA 83{}./0 7A7E-05 9.00E-15 U-235 1.70E-03 +-4.7E-04 UCI/SA 83%) 5.95E-05 9.00E-15 U-238 4.28E-02 +-B.3E-03 UCIISA 83% 7.06E-05 9.00E-15 2144068 RICHRC5011 5930, 5931 R1 NYC filters and MTNPH1AD Pb-210 2.06E-05 +-3.6E-06 UCIISA 100% 3.85E-07 6.00E-14 5932 R1 Baghouse filter and be MTNPG1AD Pb-210 8.22E-07 +-3.5E-07 UCIISA 79% 5.02E-07 6.00E-14 5933, 5934 R2 NYC filters and MTNPJ1AD Pb-210 1.73E-05 +-3.0E-06 UCI/SA 86% 4.69E-07 6.00E-14 2144069 Rl-RA..()01 5930,5931 R1 NYC filters and MTNPH1AC RA-226 B.67E-08 +-5.0E-08 UCIISA 80% 7.07E-08 9.00E-14 5932 R1 Baghouse filter and be MTNPG1AC RA-226 1.76E-07 +-6.6E-08 UCIISA 1000,{1 6.51E-08 9.00E-14 5933, 5934 R2 NYC filters and T estAmerica rptSTLRchSaSum mary2 V5.2.20 A2002 RER2 -Replicate Errol' Rntio = (S-D)llsqrt(sq(TPLJs)+,sq(TPUd»)1 as defined by lePT BOA. 1I Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the MddMda/Mdl, Totall 'llC(~!'t, CRDL, RDL or not identified by gamma scan s()ftwan~. 'l'estAmcrica Laboratories, Inc. 6 Sampie Results Summary TestAmerica Ordered by Method, Batct1 No., Client Sample 10. Report No. : 52118 Client Id Batch Work Order Parameter 2144069 RL·RA"()01 5933, 5934 R2 NYC filters and MTNPJ'IAC RA·226 No. of Results: 24 !\!\tc 'fV'C'-. \ .0 fOt{I..( )&&5& rvn 2" \ O:5C,ao3{p2.C8S- Bt< ~ t.\ ,~·v:,:" L~ J 1~ \.i { .... i , cO (£gcf <f l?81S Result +. Uncertainty ( 2:;) Qual Units 1,63E·07 +-5.0E-08 UCI/SA "::: loci41.1 ~ ~]{vo3 0. l .:::: 084 t..f ~ ~ Date: 25-Jun-12 SDG No: 45037 Tracer Yield 95% MOL CRDl RER2 5,03E-08 9.00E-14 TestAmertca R~:R2 -Replicate Error Ratio = (S-D)/lsqrt(S(l(TPlls}+sq(TPlJrl»1 as defined by ICI1T BOA. rptSTlRchSaSum mary2 V5.2.20 A2002 TestAmerica Laboratories, Inc. 7 QC Results Summary Date: 25-Jun-12 TcstAmerica Ordered by Method, Batch No, QC Type,. Report No. : 52118 SDG No.: 45037 Batch Tracer lCS Work Order Parameter Result +-Uncertainty ( 2s) Qual Units Yield Recov!'L.# Bias MOL ... RICHRC5011 2144070 BLANK ac, MTP461AA TH-228 3.34E-09 +-4.9E-09 U UC1/SA 87% 9.43E-09 TH-230 2.51 E-08 +-1.3E-08 UCIISA 87% 9.08E-09 TH-232 O.OOE+OO +-3.5E-09 U UCI/SA 87% 9.08E-09 2144070 LCS, MTP461AC TH-230 2.29E-06 +-3.5E-07 UCflSA 78% 99% 0.0 1.11 E-08 FFSR 2144071 BLANK QC, MTP471AA U-234 3.54E-07 +-1.2E-07 UCI/SA 89% 2.92E-08 U-235 -5,80E-10 +-1.5E-08 U UCIISA 89% 2.92E-08 U-238 3.83E-07 +-1.2E-07 UCI/SA 89% 2.92£-08 2144071 LCS, MTP471AC U-234 1.20E-06 +-2.7E-07 UCI/SA 89% 122% 0.2 3.47E-08 U-238 1,11 E-06 +-2.6E-07 UCI/SA 89% 108% 0.'1 347E-08 RICHRC5011 2144068 BLANK ac, MTP441AA Pb-210 5.79E-07 +-4.7E-07 U UCI/SA 62% 7.48E-07 2144068 LCS, MTP442AC Pb-210 1.39E-05 +-2.4E-06 UCI/SA 69% 153% 0.5 5.86E-07 RL·RA-001 2144069 BLANK ac, MTP451AA RA-226 2,32E-08 +-3,7E-08 U UCI/SA 100% 6.03E-08 2144069 LCS, MTP451AC RA-226 9.92E-06 t-2,1 E-06 UCI/SA 87% 100% 0,0 6.81 E-08 No. of Results: 13 TestAmerica Bias -(ResultlExpected)-l as defincd by ,:\NSI N13.30. rptSTLRchQcSum U Qual -Analyzcd for but lIot detected above limiting critcriH. Limit criteria is I('ss than the Mdc/Mda/Mdl, Total lJnccrt, ClUH" nol. or mary VS.2.20 not identified by gnmrna s{~an software. A2002 TestAmerica Laboratories, Inc. 8 lab Name: TestAmerica lot-Samp!e No.: J2E210429-2 FORM I SAMPLE RESULTS SDG: 45037 CHent Sample 10: 5930, 5931 R1 NYC filters and Denison Mine 2012 2nd Quarter Report No. : 52118 coe No.: Parameter Batch: 2144068 Pb-210 Batch: 2144069 RA-226 Batch: 214407() TH-228 TH~230 TH-232 Result RICHRC5011 2.06E-05 RL-RA-001 8.67E-08 RlCHRC5011 3.25E-08 9.36E-07 1.04E-08 Count Qual Error ( 2 s) 6.0E-07 4.6E-08 U 3.8E-08 2.0E-07 U 2.1 E-08 Total MOL, Rpt Unit, Yield RstlMDL, Uncert( 2 s) Action Lev Lc CROl{RL) RstiTotUcert Work Order: MTNPH1AD Report DB ID: 9MTNPH10 3.6E-06 3.85E-07 UCI/SA 100% (53.5) 1.87E-07 6.00E-14 (11.5) Work Order: MTNPH1AC Report DB 10: 9MTNPH10 5.0E-08 7.07E-08 UCI/SA 80% (1.2) 3.36E-08 9.00E-14 (3.5) Work Order: MTNPH1AA Report D8 10: 9MTNPH10 3.8E-08 5.19E-08 UCIISA 66% 0.63 1.13E-08 3.00E-15 (1.7) 2.7E-07 5.90E-08 UCIISA 66% (15.9) 1.54E-08 3.00E-15 (7.) 2.1 E-08 5.00E-08 UCI/SA 66% 0.21 1.09E-08 3.00E-15 0.98 Date: 25-Jun-12 CoUection Date: 5/15/20129:30:00 AM Received Date: 5/21/2012 11:00:00 AM Matrix: FILTER Ordered by Client Sample 10, Batch No. Analysis, Prep Date 6/21/1208:45 a 6/21/12 12:33 p 6/21/1208:47 P 6/21/1208:47 P 6/21/1208:47 p Total Sa Size 1.0 Sample 1.0 9 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.98906 Sample 0.9891 9 0.98906 Sample 0.98906 Sample 0.98906 Sample Primary Detector GPC31C ASC2RC ALP23 ALP23 ALP23 -------~---------.-.~-------.------ Batch: 2144071 FFSR Work Order: MTNPH1AE Report DB 10: 9MTNPH10 U-234 3.61E-02 2.1 E-03 8.6E-03 1.34E-04 UCI/SA 39% (269.4) 6/8/12 02:23 p 1.0 0.00114 ALP215 2.50E-05 9.00E-15 (8.4) Sample Sample U-235 1.42E-03 4.2E-04 5.3E-04 1.25E-04 VCI/SA 39% (11.4) 6/8/12 02:23 p 1.0 0.00114 ALP215 2.04E-05 9.00E-15 (5.3) Sample Sample U-238 3.34E-02 2.0E-03 8.0E-03 1.34E-04 UCI/SA 39% (249.2) 6/8/1202:23 p 1.0 0.00114 ALP215 2.50E-05 9.00E-15 (8.4) Sample Sample ____ • _____ HHH" .. _----------------....• ------.-..... -.. -.---.--... ----------.. -... ---.-.~--- Raao U-2341238 = 1.1 .0 tc--Gf,,-{ i &it 5 <.c TestAmerica MDClMDA,Lc· Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample U Qual-Analyzed for but not detected above limiting criteria. Limit criteria is less than the MdclMda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.Z.20 A200Z Tesu\merica laboratories. Inc. 9 Lab Name: TestAmerica Lot-Sample No.: J2E210429-2 FORM I SAMPLE RESULTS SOG: 45037 Report No. : 52118 Client Sample 10: 5930,5931 R1 NYC filters and Denison Mine 2012 2nd Quarter coe No.: Result Count Total MDL, Rpt Unit, Yield RstlMDL, Parameter Qual Error ( 2 s) Uncert( 2 s) Action Lev Lc CRDl(RL) RstlTotUcert No. of Results: 8 Comments: Date: 25-Jun-12 Collection Date: 5/15/20129:30:00 AM Received Date: 5/21 /2012 11 :00:00 AM Matrix: Analysis, Prep Date FILTER Ordered by Client Sample 10, Batch No. Total Sa Size Aliquot Size Primary Detector TestAmerica MDClMDA,Lc • Detection, Decision leve. based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchSample VS.2.20 A2002 U Qual· Analyzed for but not detected above limiting criteria. Limit criteria is less than the Mdc/Mda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. T estAmerica Laboratories. Inc. !O FORM I Date: 25-Jun-12 SAMPLE RESULTS Lab Name: TestAmerica SDG: 45037 Collection Date: 5/15/2012 10:00:00 AM Lot-Sample No.: J2E210429-1 Report No.: 52118 Received Date: 5/21/2012 11 :00:00 AM Client Sample 10: 5932 R1 Baghouse filter and be coe No.: Matrix: FILTER Denison Mine 2012 2nd Quarter Ordered b~ Client Sample ID, Batch No. Result Count Total MOL, Rpt Unit, Yield RstlMDL, Analysis, Total Sa Aliquot Primary Parameter Qual Error ( 25) Uncert( 25) Action lev Lc CRDL(RL) RstlTotUcert Prep Date Size Size Detector Batch: 2144068 RlCHRC5011 Work Order: MTNPG1AD Report 08 ID: 9MTNPG10 Pb-210 8.22E-07 3.2E-07 3.5E-07 5.02E-07 UCIISA 79% (1.6) 6/21/1208:45 a 1.0 0.9896 GPC31 B 2.44E-07 6.00E-14 (4.7) Sample Sample ------------.- Batch: 2144069 RL-RA-001. Work Order: MTNPG1AC Report DB 10: 9MTNPG10 RA-226 i.76E-07 4.6E-08 6.6E-08 6.51 E-08 UCIISA 100% (2.7) 6/21112 12:35 p 1.0 0.9896 ASC1RH 3.13E-08 9.00E-14 (5.3) 9 9 Batch: 2144070 RICHRC5011 Work Order: MTNPG1AA Report DB iD: 9MTNPG10 TH-228 4.65E-08 U 5.6E-08 5.6E-08 8.64E-08 UCI/SA 52% 0.54 6/21/1208:47 p 1.0 0.9896 ALP21 2.47E-08 3.00E-15 (1 .7) Sample Sample TH-230 2.5SE-OS 1.2E-06 5.3E-06 6.32E-08 UCI/SA 52% (402.9) 6/21/1208:47 P 1.0 0.9896 ALP21 1.37E-08 3.00E-15 (9.6) Sample Sample TH-232 3.43E-07 1,3E-07 1.SE-07 6.32E-08 UCI/SA 52% (5.4) 6/21112 08:47 p 1.0 0.9896 ALP21 1.37E-08 3.00E-15 (4.5) Sample Sample -----_ ...... __ .. --------------_ .. _------_ ....• --_ .. "---"._---_._-_.",--------- Batch: 2144071 FFSR Work Order: MTNPG1AE Report DB 10: 9MTNPG10 U-234 3.44E-03 4.3E-04 7.7E-04 5.70E-05 UCI/SA 92% (60.4) 6/8/1202:23 p 1.0 0.00108 }\LP213 1.06E-05 9.00E-15 (9) Sample Sample U-235 1.18E-04 7.9E-05 8.2E-05 5.31 E-05 UCI/SA 92% (2.2) 6/8/1202:23 p 1.0 a.OOi0a ALP213 8.68E-06 9.00E-15 (2.9) Sample Sample U-238 3.31 E-03 4.2E-04 7.4E-04 5.70E-05 Vel/SA 92% (58.) 6/8/12 02:23 p 1.0 0.00108 ALP213 '1.06E-05 9.00E-15 (8_9) Sample Sample --_ .. _------------- Ratio U-2341238 = 1.0 .. 00 (;$iCf 4 erJ'-:r·,s TestAmerica MDClMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Vield, and Volume. rptSTLRchSample V5.2.20 A2002 U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is tess than the MdcIMda/Mdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. TestAmerica Laboratories. rnc. If Lab Name: TestAmerica LotwSample No.: J2E210429-1 Client Sample m: 5932 R1 Baghouse filter and be Denison Mine 2012 2nd Quarter FORM I SAMPLE RESULTS SDG: 45037 Report No. : 52118 cae No.: Result Count Qual Error ( 2 s) Total MDl, Rpt Unit, Yield RstlMDl, Parameter Uncert( 25) Action Lev Lc CRDL(RL) RstiTotUcert No. of Results: 8 Comments: Date: 25-Jun-12 Collection Date: 5/15/2012 10:00:00 AM Received Date: 5/21/201211:00:00 AM Matrix: Analysis, Prep Date FILTER Ordered by Client Sample ID, Batch No. Total Sa Size Aliquot Size Primary Detector TestAmerica MDClMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency., Yield, and Volume. rptSTLRchSampie U Qual -Analyzed for but not detected above limiting criteria. limit criteria is less than the Mdc/MdalMdl, Total Uncert, CRDL, RDL or not identified by gamma scan software. V5.2.20 A2002 TestAmerica Laboratories. Inc. 12 Lab Name; TestAmerica Lot-Sample No.: J2E210429.3 FORM I SAMPLE RESULTS SDG: 45037 Report No. : 52118 Client Sample 10: 5933,5934 R2 NYC filters and Denison Mine 2012 2nd Quarter coe No.: Parameter Batch; 2144068 Pb-210 Batch: 2144069 RA-226 Batch: 2144070 TH-228 TH-230 TH-232 Batch: 2144071 U-234 U-235 U-238 Result RICHRC5011 1.73E-05 RL-RA-001 i .63E-07 RICHRC5011 8.57E-08 1.86E-05 5.98E-08 FFSR 4.15E-02 1.70E-03 4.2BE-02 Count Quai Error ( 2 s) 6.3E-07 3.9E-08 5.2E-08 7.SE-07 4.3E-08 1.6E-03 3.3E-04 i.7E-03 j 08&0 3 &>2.085'- Total MOL, Rpt Unit, Yield RstlMDL, Uncert( 25) Action Lev Lc CROL(RL) RstlTotUcert Work Order: MTNPJ1AD Report DB 10: 9MTNPJ10 3.0E-06 4.69E-07 UCI/SA 86% (36.9) 2.28E-07 6.00E-14 (11.6) Work Order: MTNPJ1AC Report DB 10: 9MTNPJ10 5.0E-08 S.03E-08 UCI/SA 95% (3.2) 2.37E-08 9.00E-14 (6.4) __ • ___ ••••••• ____ ••••••••••••• _ •• ____ .. _ •• ,_ ........... __ ........... ____ M ____ Work Order: MTNPJ1AA Report DB iD: 9MTNPJ10 5.5E-08 3.61E-08 UCI/SA 90% (2.4) 7.36E-09 3.00E-15 (3.1) 3.4E-06 3.49E-08 UCIISA 90% (534.8) 7.10E-09 3.00E-15 (11.) 4.4E-08 3.49E-08 UCI/SA 90% (1.7) 7.10E-09 3.00E-15 (2.7) .----_ •... _-_ .. _ .......... -----... -... _-.. _----,-..• '._- Work Order: MTNPJ1AE Report DB ID: 9MTNPJ10 8.1E-03 7.4 7E-05 UCI/SA 83% (554.7) 1.S2E-05 9.OGE-iS (10.3) 4.7E-04 5.9SE-05 UCi/SA 83% (28.6) 7.61E-06 9.00E-15 (7.3) 8.3E-03 7.06E-OS UCI/SA 83% (605.7) 1.32E-05 9.OOE-iS (10.3) --_._._ ....... _.¥ •. _ •• _._._ .... _ .... __ .. _ .. _. __ .... ----- Ratio U-2341238 = 1.0 Date: 25-Jun-12 Collection Date: 5/16/2012 7:45:00 AM Received Date: 5/21/2012 11 :00:00 AM Matrix: FILTER Ordered by Client Sample ID, Batch No. Analysis, Prep Date 6/21/12 08:45 a 6/21112 12:33 p 6/21/1208:49 P 6/21/1208:49 P 6/21/1208:49 P 6/8/1202:23 p 6/8/1202:23 p 6/8/1202:23 p Total Sa Size 1.0 Sample 1.0 9 1.0 Sample 1.0 Sample 1.0 Sample Aliquot Size 0.98793 Sample 0.9879 9 Primary Detector GPC31D ASC3RA -.-...... --.- 0.98793 ALP116 Sample 0.98793 ALP116 Sample 0.98793 ALP116 Sample ------- 1.0 0.001 ALP216 Sample Sample 1.0 0.001 ALP216 Sample Sample 1.0 0.001 ALP216 Sample Sample TestAmerica MDClMOA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficifmcy, Yield, and Volume. rptSTLRchSampie U Qual -Analyzed for but not detected above limiting criteria. Umlt criteria is less than the MdclMdalMdl, Total Uncert, CROl, RDl or not identified by gamma scan software. V6.2.20 A2002 TestAmt:rica Laboratories. Inc. 13 Lab Name: TestAmerica Lot-Sample No.: J2E210429-3 Client Sample tD: 59331 5934 R2 NYC filters and FORM I SAMPLE RESUL T5 SOG: 45037 Report No. : 52118 coe No.: Date: 25-Jun-12 Collection Date: 5/16/2012 7:45:00 AM Received Date: 5/21/2012 11 :00:00 AM Matrix: FILTER Den ison Mine 2012 2nd Quarter Ordered by Client Sample 10, Batch No. Result Count Parameter Qual Error ( 2 s) No. of Results; 8 Comments: Total MOL, Rpt Unit, Uncert( 2 s) Actio n lev Lc Yield Rst1MDL, CRDl{RL) RstlTotUcert Analysis, Prep Date TestAmerica MDCJMDA,Lc -Detection, Decision Level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. Total Sa Size Aliquot Size Primary Detector rptSTLRchSample U Qual -Analyzed for but not detected above limiting criteria. Limit criteria is less than the MdcfMda/Mdl, Total Uncert, CRDL, ROL or not identified by gamma scan software. V5.2.20 A2002 TestAl11crica Laboratories. Inc. 14 FORMU BLANK RESULTS Date: 25-Jun-12 Lab Name: TestAmerica Matrix: FILTER Parameter Result Qual Batch: 2144068 RICHRC5011 Pb~210 5.79E~07 U Batch: 2144069 RL~RA-001 RA-226 2.32E-08 U Batch: 2144071 FFSR U-234 3.S4E-07 U-235 -S.BOE-10 U U-238 3.83E-07 Batch: 2144070 RICHRC5011 TH~228 3.34E-09 U TH-230 2.51 E-08 TH-232 O.OOE+OO U Count Error ( 2 s) 4.6E~07 3.6E-OS 1.0E-07 1.SE-08 1.1 E-07 4.9E-09 1.3E-08 O.OE+OO -.---... ~---------- No. of Results: 8 Comments: 6 cCt/cD I 3 {}'1cf;' SDG: 45037 Report No.: 52118 Total MDL, Rpt Unit, RstlMDL, Analysis, Total Sa Aliquot Uncert( 2 5) lc CRDL Yield RstiTotUcert Prep Date Size Size Work Order: MTP441AA Report DB 10: MTP441AB 4.7E-07 7ASE-07 UCI/SA 62% 0.77 6/21/1208:46 a 220.42 220.42 3.65E~07 6.00E-14 (2.5) Sample Sample Work Order: MTP451AA Report DB ID: MTP451AB 3.7E-OB 6.03E-08 UCI/SA 100% 0.39 6/22/1207:40 a 220.42 220.42 2.8BE-08 9.00E-14 (1 .3) 9 9 ... __ ._-------- Work Order: MTP471AA Report DB iD: MTP471AB 1.2E-07 2.92E-08 UCI/SA 89% (12.2) 6/8/1203:13 p 1.0 1.0 4.77E-09 9.00E-i5 (6.) Sample Sample 1.5E-08 2.92E-08 UCI/SA 89% -0.02 6/8/1203:13 p 1.0 1.0 4.77E-09 9.00E-i5 -0.08 Sample Sample t2E-07 2.92E-08 UCI/SA 89% (13.1 ) 6/8/12 03: 13 p 1.0 1.0 4.77E-09 9.00E-15 (6.2) Sample Sample Ratio U~2341238 = 0.9 ~~--------~.------_._---_.------------- Work Order: MTP461AA Report DB ID: MTP461AB 4.9E-09 9A3E-09 UCIISA 87% 0.35 6/22/12 03:29 a 220.42 220.42 2ASE-09 3.00E-15 (1.4) Sample Sample 1.3E-08 9.08E-09 UCI/SA 87% (2.8) 6/22/1203:29 a 220.42 220.42 2.36E-09 3.00E-1S (3.7) Sample Sample 3.5E-09 9.0BE-09 UCI/SA 87% O. 6/22/12 03:29 a 220.42 220.42 2.36E-09 3.00E-15 O. Sample Sample ------------_._--_. - ------.--.-------~--.,,----,------ TestAmerica MDCIMDA,lc. Detection, Decision level based on instrument background or blank, adjusted by the sample Efficiency, Yield, and Volume. rptSTLRchBfank l.l QU(-Il-Analyzed for but not de-tected above limiting criteria. Limit o-ite-ria is less than the MdcJMda/Mdl, Totallincert, CRDL, RDL or !lot idelltified by gamma scan software. V5.2.20 A2D02 TestAmerica Laboratories, fnc. l5 Primary Detector GPC32A ASC6RD ALP217 ALP217 ALP217 ALP117 ALP117 ALP117 Lab Name: T estAmerica Matrix: FILTER Parameter Result Qual Batch: 2144068 RICHRC5011 Pb-210 1.39E-05 Batch: 2144069 RL-RA-001 RA-226 9.92E-06 Batch: 2144071 U-234 1.20E-06 U-238 1.11E-06 Batch: 2144070 RICHRC5011 TH-230 2.29E-06 No. of Results: 5 Comments: Count Error (2 s) 6.7E-07 2.3E-07 1.9E-07 1.BE-07 FORMU Les RESULTS Total Report Expected Uncert(2 s) MDL Unit Yield Expected Ul1cerl Work Order: MTP442AC Report DB 10: MTP442CS 2.4E-06 5.86E-07 UCI/SA 69% 9.04E-06 1.S2E-07 Rae limits: 75 125 Work: Order: MTP451AC Report DB lD: MTP451CS 2.1 E-06 6.B1 E-OB UCI/SA 87% 9.92E-06 i.01E-07 Rae Limits: 75 125 Report DB ID: MTP471 CS 2.7E-07 3,47E-08 UCIISA 89% 9.82E-07 5.94E-09 Ree Limits: 75 125 2.6E-07 3.47E-08 UCI/SA 89% 1.03E-06 6.22E-09 Rac Limits: 75 125 .. ------.. ------.-Work Order: MTP461AC Report DB ID: MTP461CS 1.2E-07 3.5E-07 1.11 E-08 UCI/SA 78% 2.31E-06 2A1E-08 Rec Limits: 75 125 T estAmerica Bias -(Result/Expected)-1 as defined by ANSI 1'113.30. rptSTLRchLcs VS.2.20 AZ002 TestAmerica Laboratories. Inc. 16 Date: 25-Jun-12 SDG: 45037 Report No. : 52118 Recovery, Analysis, Aliquot Primary Bias Prep Date Size Detector 153% 6/21/1206:50 p 221.28 GPC318 0.5 Sample 100% 6/21/12 12:31 p 221.28 ASC7UA 0.0 9 122% 6/8/1203:14 p 1.0 ALP218 0.2 Sample 108% 6/8/1203:14 p 1.0 ALP218 0.1 Sample 99% 6/22/12 03 :29 a 221 .28 ALP118 0.0 Sample ~ ;; 3 ~ n' Cj~ k"t 0-o @ ~ ~. o --.J I ~-;~S;>:~1+ ;,'l;'tl;~~~~:"·:~:::~/'~~~¥§~:,'~l{~~~}t :'~0 }1!~tt}?! Chain of Custody Record TAL4124 (1007\ elisor Temperature on Re"vGipt __ _ Drinking Water? Yes 0 No 0 < ! I PrQ~Qt tliBM.a~r Tetco it!Dean Kit(:;hen :~r39~.~~t_6~~S~~"-~-=;:;;.;::_.....~;L~j~~~;:~;;;.-- i American Fork \ lut ___ t.&.4QQ.1 .. _ ... ,_., .... "Jscouchristensen.o..rrinpafmer . Protect Neme Md L«;a/fO(t (State) Denison M ine 2012 2nd Quarter I Oamer/I/l);a.ybiTi Number CcntroctlPlJrcfl~fXJ Oroer/Qllctc No. e merlca THE LEADER IN ENVIRONMENTAL leSTfNG . llk!if! j I ) 5/15.1612012 I Lab Number I Arlarysfs (Attach fist If mora space is f'lseded) 1'''11 May£)( PresewatlYes! ." o:! U)' t:jll r t.Cl:i8frrOf.CUS1£d'l.NUmbet--.j . Jj : I Page Qf speciaJ!nsUuct~nsl C~~~onsofRe~pt t . Container~ 8. ! ~ ! i '1 o~ . '-.~-'"I I : "'! . ~ ~ ; ~t ~ [ ~ ~i fl~5!f.~~~~~~~~j!~~!i~:11~i;~-i !:i, i![J ~I ~/ i~~ tlrJ~j t+:--4-t-.--+ ;:-' -i!-' --------- j I I Possible Hazt!rd IdrmtitlCation o Non-Hazl1Jti 0 Flammahfe o Skirr irritant o PoisonS ium Around rime Figquired o 24~fS 0 48H<Jff$ 0 7 Days-o 14D-ays-o 21D:zys 1.. Re(ifJ~flJed 8y >: ( ~. (1'----, Z. Re/lt1qiiiShsd By =-- 3. Refinq!"'ished 8y Comments When Complete Email to:DeanorPaultetco@tetco-ut .com J I I , TFme 1 l1lSTRiB7jtlof,{:W"'fff!:-=Relurl7sdtc Client \"Jim Report; CANAF1V~StEys with the Samp,,"; FiNK ~ F!efd Capy "I.J I tJ '1 . r-r f I [2t Disposa{ By Lab o Archiye rer ___ Morrlnr; ~ 3. ne--wCirreri Sy fir fee may be OiSSFJ$S$d if S!JmPf~s ere retf!irwd fOngG' thl,ln 1 mQnth) !4vj.z Date. I Tlffie I :S-.Z/.JZ I IIO(j I DaW ! rim~ I I I DEte [ Time TestArnerica ~ n lE L"I\()a-~ IN t':NvIHClNMENTAL ff!$Tlt4t-, 8mnplc Chccl{-in List . f' G 1,1 _·t._·' __ I_I_D_V Container GM Screen Result: (Airlock)-0 i, Illitia'tc, . Sample GM Screen Result (Sample Receiving) __ 10_ .. _CIJllitialsC!(. Date/Time Received: Client: D~tN SDG #: if <)Q_'{_L_NA [] SAP #: _______ . ________ . __ NA{f!:/(- Lot Number: T2DI QL/Z( Chain of Custody # -!J L~··--·~~-------------.----.-.-----...... --.--.. ---- Shippillg Container ID: __________ NA teJ fC. Air Bill Number: NA~}( Samples received inside shipping container/cooler/box y es ~ K1 Continue with 1 t11rough 4. lnit@} appropt'iate response. J. Custody Seals on shipping container intact? 2. Custody Seals dated and signed? 3. Cooler temperature: 4. Vermiculite/packing materials is No [ J Go to 5, add comment to #16. Yes [ No I: Ycs [ No [ __ ~_OC NA[ Wet [ No Custody Sea.l lQ '6' No Custody Seal ((j~; ? NA~.,i~ DrytC/~- It.em 5 through 16 for samples. Initiill appropriate response. 5. 6. 7. 8. 9. 10. 11. Chain of Custody record presont? Yes G' ~ No [ ] Number of samples rcceive~ (Each s· mple may contaitllllultiple bottles): _____ 3_.~ ______ ~ _____ ... __ ._ ..... _. __ _ . t f t /rJ r f t,/{?/:/f K£')t I:>~r\ Containers received: ___ \(,?__ X. r t-, A ~: __ ~___ -_). --------_ ... -_._- Sample holding times exceeded? Samples have: ______ tape ____ custody seals Matrix: A (FLT, \-Vipe, Solid, Soil) 01C~s (Air, Niosh 7400) Sa~1?les: LL(.~·e in good condition __ are broken ___ Other _ .. __ . _______ . ___ . ___ _ NA[ Yes [ __ hazard labels _'_appropriate sample labels __ I (Water) _~T (Biological, Ni~63) _. _are leaking No (21<[ __ ._have ail" bubbles (Only for samples requiring no head space) 12. Sample pH appropriate for analysis requested Yes [ ] No [ ] NA {l> Itf-. (If acidification is necessary, then document sample rD, initir pH, amount of HN03 added and pH after addition on table overleaf) RPL ID # of preservative used : ______ 1(; 0 ______ .. ___ ._. _______ ... ______ ~ ___ ._ .. _~ ______ _ Yes [ ] NolC/(f 13. Were any anoma1ies identified in sample receipt? Ole Description of anomalies (include sample numbers): NA [ J ________ ~. ____ ._. ___ _ 14. LS-023, Rev. 15) 07/11 See over for additional information. TestAmerica Lab{)ratories. Inc. 18 TestArnerica ~lHt tEADen iN UNVtn.ONMt:N-rAL 1'~~S'T1N(~ 15. 16. Sample Location, Sample Collector Listed on COe? * *For documentation only. No cOlTective action needed. Additional Infotmation: _____ _ Yes [' ] N 0 lCY~ ---_.,._-_ ... -------.---.--~----- ._---_._-_._. -_._--_ .. _----_ ... -._---_ ..... _._ ... ---.. -._- ----.-~--.--.--.--.------------... -.-----.. [ I] ClienUCourier unpack cooler. Sample Custodian: __ """'=-___ --..:~ s: L t 1'(-· Date: __________ . ____ ._._._ ... __ .. ____ . ______ ..... ____ _ Client Informed on ... _ by __ .. _. ____ .. _ .. ______ Person contacted._ ... ___ ._ .. __ ...... _ ......... _. __ _ )~f No Rction necessary; proce~s as is projectMan.ger_~~-Date cS ,22 -(0 ____ . __ / --- j f ____ _ \~v/ M \ \ --------~~t:T---.----.-----. A ~J~I f----------+--/-,->,.q4j-,--/.-F----.. ------.... --.--I-----------+-----/-~~----4"j.<-+.I/'-----If-----__ .. -__ .-_-- 1/ I p// i---~-----_+---+--I-----+_----_I_---------I_--'td'L...f-+__----.. --· --.---. --~/ I\~j i----------------~--~~-~-----.r_-----~----------~~~~-_+--.. -----~.---.-J/ \ /H'''/ 1__--------."k~I__--_t-~---_I_--~_I___'--------'\_-----l\_._I_---l_--~-____J..-.---. ---.-. \ A"!'/ \ \j '\ \ V ~ d\ 7 l/-+---·-1-------- f---------\-~-_fl_----1_----1r---__;F---:>.\...----=-+-~--;;---fl------+-----"-.. -....... ----.. -.. - Cvt)A / f \" r~/ 1------rrh~_f___+----~-----1_--_t\·I----.JT\--~~-~L-.I------·---------.------ !-/)// \/ ,,} ~ / I LS-023, Rev. 15; 07/11 See over for additional inf()rrnution. 'restArnerica Laboratories, Inc. 19 APPENDIXD North Yellow Cake Scrubber Figure 1. Facility Schematic Representation YeHow Cake Dryer Baghouse Figure 2. Facility Schematic Representation Production and Control Equiprrlent Data North Yellow Cake (Scrubber Flow Rates) Yellow Cake Dryer Baghouse (11 barrels filled during test) o Facility: Denison Mines t (X t y Stack Identification: Yellow Cake Baghouse l~0~f IF""" g [3 ex; Distance upstream from next disturbance, inches 57" -------------------- ~: Distance downstream from last disturbance, inches 454" y: Distance of Sample Level to Ground, feet 6Y 0: Stack Inside Diameter, inches 1611 -------------------- Estimated Moisture, percent 0-2% Estimated Temperature, of -------------------125 Estimated Velocity, fpm 1,400 2 r Process l Type: Number of Ports ContmlUnit Type: Baghouse ~ Figure 2. Facility Schematic Representation Yello\v Cake Processing Facility: Denison Mines t a t y ! Stack Identification: North Yellow Cal<e Scrubber 1+-0 ~1 I fJ t a: Distance upstream fi'om next disturbance, feet B: Distance downstream from last disturbance, feet y: Distance of Sample Level to Grotmd, feet 0: Stack Inside Diameter, inches Estimated Moisture, percent Estimated Temperature, of 9.5' ------------------- 9 _' .) 65' ------------------ 18" ------------------ 8-15% 100-120 ------------------- Estimated Velocity, fplll 1,100 Control Unit Type: Scrubber N umber of Ports 2 ~ Figure 1. Facility Schematic Representation Process Type: YeHow Cake Processing I .. ,-,,' , Denison Mines Process Data 1 I Source: North Yellow Cake Date: "g ~ ) I S--/ 1--<-. Scrubber Flow GPM Time #1 #2 ·~44.v i.~·· i·{ I () : 3 u (\ : t) b C' ~ ?5"' . <"" rf t .; .. ./ r----------+------~--_+----------~~----------.- i .-3 \ S, / It.) v f (p 3 { ~. 0 0 .... . C:~ ~. I 0 0 0 'S / .. , ~':7 f ! . f ' I 'S5 . () (-\ . .,c.. 1 v (~ . , ,~, j Denison Mines Process Data I I Source: North Yellow Cake Date', c .. -. /1 '.'-/1 . .., ) () / (- Scrubber Flow GPM Time #1 0 0 r ; c) l.J (j) , C'r \ i \ -" I " -. '7 V L() t ~~---------+--------~--~----------~~--------------lL (' C'-"" /~! J f \ \.1) ~'------------r------------~----------~~--------,--~ () c) (p.l> ~--------~-+--------~--~------------~-------------c...:-I ? '--,J, ) c ...... -~ APPENDIXE Calibration of the console dry gas rneter(s), pitot tubes, nozzles diameters, and temperature sensors were can-ied out in accordance with the procedures outlined in the Quality Assurance Handbook. The appropriate calibration data are presented in the following pages. The nozzle calibrations are recorded on the first page of the field data sheets. Figure 3 Schen1atic of1\1ethod 5/114 Sampling Train Meter Box Calibration Data and Calculations Forms Post-test Dry Gas Meter Calibration Data Forms Type S Pitot Tube Inspection Data Sample Box Ten1peratlrre Sensor Calibration E Temperature Sensor ~ I ~ 'N Probe I mpingerTrain Optional, May 8e Replaced By An Equivalent Condenser r Type S Pilot Temperatura Tube Sensor Temperature sensor~ Gooseneck 1. . .. .,--...Il...-------,r. ________ _ 1 Temperature Sensor Nozzle . ..t-eat Traced ~ . ~jmd w . / PrObe ---,. / Type S Plto! Tube ~ Stack Wall Manometer (Dry Gas . \ Meter ) ~J Air-Tight Pump Figure 3 Schelnatic of Method 51114 SatnpIing Train I (vacuum ~une m Vacuum '\ , ,11' Gauge ) ~ METHOD 5 DRY GAS METER CALIBRATiON USING CRITICAL ORIF!CES 1) Select three critical orifices to calibrate the dry gas meter I",hich bracket the expected operating range. B G G 2) Record barometric pressure before and after calibration procedure. 3) Run at tested vacuum (from Orifice Caltbration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the cells, YELLOW cells are calculated, METER SERIAL #: CRITICAL ORIFICE SET SERIAL #: K' TESTED FACTOR VACUUM RUN# (AVG) (inHg) 5.280 7S 5.278 75 5.546 75 5.205 75 5.240 75 5.246 75 5.50t 75 5.509 75 5.513 75 - USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS; 16 an 82 80 81 64 81 83 85 84 1\6 88 86 87 86 87 89 87 84 85 87 86 87 89 INITIAL DOM AVG 73.75 76 78.50 80,50 112.50 84,00 86.00 86,50 88.00 Facility FINAL 25.3(j ELAPSED T!ME(MIN) e ENViRONMENTAL SUPPLY COMPANY AVGIPb•r) 25.3 [§ 2.,00 2.00 uo 1.20 1.20 Pre Calibration 2012 ill!§. 4.4342 lli@ !dill 4,3282 4,322S 4,5047 gQl.f 4.4981 IF YVARIATION EXCEEDS 2.00%, ORIFICE SHOULD BE RECALlBRATED 1 4.4515 0.999 4.4515, 1.004 4.6740, 1.Q.Q! AVG= 1.004 -0:.22 4.3631 .!.Jill 4.3631 1,,008 4.3631 1.009 AVG= i.Q.Q! Qd§. 4.622~ 1.004 4.5229 ~ 4,5229 1.006 AVG= ~ -0.15, The following equations are used to calculate ihe standard volumes of air passed through the DGM, V m (sId), and the critical orifice, V" (std). and thi; DGM calibration factor, y, These equations are automaticallycafculated ill the spreadsheet above. .AVERAGE DRY GAS METER CAUBRA TION FACTOR, Y = I 1,0001 (1) (2} (3) Vm",,,d, =: K J *Vm* Pbar+('-.\f-{ /136) Tm--' Pbar * ~ I· 'cr,,.</ " ~"I:'* JTamh = Net volume of gas sample passed through DGM, corrected to standard conditions K, :: 17,64 'R/in, Hg (English), 0.3858 QKJmm Hg (Metric) T m:: Absolute DGM avg. temperature (OR -English, OK -Metric) '" Volume of gas sample passed through the critical orifice, corrected to standard condilions Tan,," Absolute ambient temperature ("R" English, of(" Metric) K' = Average K' factor from Critical Orifice Calibration f. 'CI:.,!,f' r= Vm"Ui; '" DGM calibration factor Pre Calibration 2008 AVERAGE ~H@ =l -1:64'1 -I L'.H@= ( 0,75 e)2 L'.H (Vm(std) Vcr(std) V", Temperature Sensors Reference In Out OF OF OF 34 67 202 35 68 203 35 68 203 ~ ~ 1.721 .1.&§i 1MI ~ ~ 1MI 1.S42 METHOD 5 DRY GAS METER CALIBRATION USING CRfTICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range, 2} Record barometric pressure before and after calibration procedure. G G G 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet 4) Record data and information in the c;nE:a,j cells, YELLOW cells are calculated, METER SERIAL #: CRITICAL ORIFICE SET SERIAL #: K' TESTED FACTOR VACUUM RUN # (AVG) (In Hg) 5.343 7:0 5.342 7-0 3 5.347 10 5.151 74 5.157 74 5.502 74 5.t51 75 2 5.144 75 5.150 75 USING THE CRfTlCAL ORIFICES AS CALIBRATION STANDARDS: 77 7'8 71 71l 79 71 19 80 71 74 76 70 76 74 71 74 7·6 71 73 75 71 75 76 71 76 78 71 71 71 71 71 71 71 71 71 71 INITIAL DG~ AVO 74.25 74.75 75.25 72..15 73.00 73.00 72.50 73.25 74.00 FINAL 25.55 J.#i~ -.I!Ji@:~;:::~;'f: ENVIRONMENTAL SUPPLY COMPANY AVG[P"",) 25.55 3.U')! 3.02 3.02 1.20 1.20 1.20 2012 Pre-CaHbration Console 8 4.5535 4.5441 4.5442 4.3753 4.3733 4.6712 4.3581 4.3560 ~ IF YVARIATION eXCEeos ... 00%, ORIFICE SHOULO BE RECALIBRATEO 1 4.5166 ~ 4.5166 0.994 4.5166 ~ AVG= !h!!.l!l -0.89 4.41 \)4 1.003 4.4104 .1.Q..Q1 4.7044 1.007 AVG'" 1,007 Q,ll 4.3849 1.004 4.3849 .1.Q..Q1 4.3849 1.007 AVG'" " •. 006 0.36 1.773 1.771 1.769 ~ 1..§E 1.657 1.643 1.641. 1.G39 The following equations are used to calculate the standard volumes of air passed through the DGM, Vm (std), and the critical orifice, V" (sid), and the DGM calibration factor. Y_ These equations are automatically calculated in the spreadsheet above, AVERAGE DRY GAS METER CALIBRATION FACTOR, Y= I 1.002 (1) VIII(.<ld) = K, * Vm" (2) Vcr K '" ~!:~!;~~,::;;.- -.!Tumh (3) ),. = Vlllj.-la' = Net volume of gas sample passed through DGM, corrected to standard conditions K, " 17,64 QR/in. Hg (English), 0_3858 "Klmm Hg (Metric) To, =: Absolute DGM avg, temperatura ("R -English, QK · Metric) = Volume of gas sample p.assed through the critical orifice, corrected to standard conditions T,~o '" Absolute ambient temperature CR . English, Gt< -Matrici K' = Average K' factor from Critical Orifice Calibration = OGM calibration factor AVERAGE ~H@ =1 1.690 ilH@ ;: ( 0.75 e )2 !lH (V m(std)) V.,(std) V," Temperature Sensors Reference In Out "F OF OF 32 33 33 72 201 73 202 73 203 Console 8 Pre-test METHOD 5 DRY GAS METER CALIBRATION USING CRITiCAL ORifiCES ~ G;"";~~ 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range. 2) Record barometric pressure before and after calibration procedure. ENVIRONMENTAL SUPPLY COMPANY 3) Run at tested vacuum (from Orifice Calibration Report), for a period of time necessary to achieve a minimum total volume of 5 cubic feet 4) Record data and information in the GREEN cells, YELLOW cells are calculated, RUN # K' TESTED I FACTOR I VACUUM (AVGJ I (in Hg) METER SER!AL #:1-1 ~---l CRITICAL ORIFICE SET SERIAL #:j 1453S EQUIPMENT 10 #: .0 I II 111 .0 .0 G:rn §g 87&.147 OAi311 1~ 871. •. 50.6 ·881J~99 876.747 Q.53"t7 13 881.9$9 887.268 0.5317 13 I.:l ...........• ,. i . ,( , .'. i LJ 2 r-:l1~ ~ LJ : l=t=j t=±=j USING THE CRITICAL ORIFICES AS CAL!8FtA.T!ON STANDARDS: 5.241 5.252 5.269 .0 .0 .0 70 74 74 7.1 78 70 74 7.1 78 82 10 77 80 82 84 1---1 C-r -j ]j INITIAL DGM AVG o o 0.00 75.75 77.75 80.75 0.00 0.00 0.00 Facility FINAL 25:15 ELAPSED TIME (MIN) e AVG (Pbar) 25.15 §§ L§ 1.20 1.20 7.5\1 7.5Q 1.20 §§ Dennison Mines 4.3577 4.3506 4 •. 340.5 IF Y VARIA nON EXCEEDS 2.00%, ORIFice SHOULD BE RECALtBRATED 1 AVG= 4 .. ~577 MOO 4.3577 1.J!!!g 4 .. 3577 1.004 AVG= ~ 0.00 AVG= The following equalions are used to calculate the standard volumes of air passed through the DGM, V In (std), and the critical orifice, V Of (sId), and the DGM calibrafion factor, Y. These equations are automatically calculated in the spreadsheet above, AVERAGE DRY GAS METER CALIBRATION FACTOR, y.., I 1.002 (1) (2) (3) Vm(Jld) = Kl * Vm * Phar + (6H /13.6) Tm Pbar.-:~_ Vcr(,.td ) = K '*-"ffa;nb :: Net volume of gas sample jJ8!lsed through DGM, corrected to standard conditions K, = 17,64 °Rlin. Hg (English), 0.3858 °KJmm Hg (Metric) T m = Absolute DGM 8Vg, temperature (OR -English, OK -Metric) = Volume of gas sample passed through the critical orifIce, corrected to standard conditions Tamb = Absolute ambient temperature COR -Engli.sh, OK -Metric} K' '" Average K' factor from Critical Orifice Calibration y= = DGM caHbration factor Vm("d) Pre Calibration 2008 AVERAGE ~H@ =1 1.055 6H@=( 0,75 e )2 6H (.Vm(std») Vcr(std) Vm ' Temperature Sensors Reference In Out OF Of OF 34 35 35 67 68 68 202 203 203 1.663 1.656 1.£147 METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES 1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range, 2) Record barometric pressure before and after calibration procedure. ;5) Hun at tested vacuum (tram Ontlce Gallbratlon Keport). tor a penoo ot time necessary to achieve a minimum total volume of 5 cubic feet. 4) Record data and information in the GREEN cells, YELLOW cells are calculated, METER SERIAL #:G;[J CRITICAL ORIFICE SET SERIAL #:~ EQUIPMENT 10 #: K' TESTED FACTOR I VACUUM I RUN # I (AVG) . (in Hg) o : L~·OOU ... .!2 ... _ C..S8DS 12 , 0.S808 12 229 ... 2:10' 234.541 234.547 239.ea3 ! 2.39~~_!~:~~~ 5.337 . 5.336 5.347 70 70. 7Q 72 . 75 77 75 7'1 77 71 78 12. 71 72 72 D:E:E~ D:EE~ .0 .0 .0 '~-111 · fl USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS: .0 .0 .0 I· •. ··' [111 INITIAL DGM AVG 72.25 73.75 74.75 0.00 0.00 0.00 0.00 0.00 0.00 FINAL 25.15 ELAPSED TIME (MIN) 6 AVG (Pba,) 25.15 S;OQ 2 . .10 5;00 2.10 6.00 2.10 §§ §§ 4 . .47aS 5.:ill2 4.4659 .1\ ,?U\f \j -----a&;Zi Dennison Mines IF Y VARIATION ExceeDS 2.00%. ORIFICE SHOULD BE RECALIBRATED 1 4.4f137 0.9.97 1.71}1 4.4637 1.QQQ 1.786 ~ 1.000 1..:.lli. AVO'" ~ 0.00 AVO:;: AVG= The following equations are used to calculate the standard volumes of air passed through the DGM, Vm (std). and the critical orifice. Vcr (Sid). and the DGM calibration factor. Y. These equations are automatically calculated in the spreadsheet above. AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = I 0.999 (1) (2) (3) Vm(S/d} := K, * Vm * Pbar + (Mi /13 .6) Tm = Net volume of gas sample passed through DGM, corrected to standard conditions K\ '" 17.64 oR/in. Hg (English). 0.3858 °Klmm Hg {Metric} Pbar * e Vcr(SId) = K'* .JTamb Vcr'Sfd) Y::; _'_ L Vm(sid) T m = Absolute DGM avg. temperature (R -English. oK -MetriC) = Volume of gas sample passed through the critical orifice. corrected to standard conditions T atr.b ::: Absolute ambient temperature (OR -English. OK -Metric) K' "" Average K' factor from Critical Orifice Calibration :: DGM calibration factor AVERAGEl\H@"'1 1.786 l\1i@:;: (O~75 e )2 l\H (Vm(std}) Vc,(std) Vm Temperature Sensors Reference In Out OF 33 67 121 OF 34 86 120 OF 34 66 120 Console 8 Post-test Dal~, Dt Type S Pilot Tubt: Inspect ion Data "') ., \1..~' I \ \ l<' (" PilOt Tub.:: Id(:t1lificatint'l ~.-::J~_"' __ , ___ . __ ._ p~ == • l.{ t;; () in, ~------~~-------- Ill, Ul <: 10" (J'1 <. 10· Cl : = __ --'-__ ~ Z ~O,125 ill, \V s 0,03125 in w~ 00 &1 W> 3 incheS W"'-(p '/ ;"~. z> 3/4 inch l'""' , I". 'ij The PIlOt tube meets the spccilic3l10llS for a cali bration factor <lfO g,r' _'I.e..!:> . StIck Rdercllcl;' Temperatur~ Source (1vkdl\Jrn) ~~ ___ .Contlnulty l-!e:lt Check 2~S leE WATER BOIL \VATER SILICONE OIL ~========~~=---Tcnwer(lLll;.:,cre,:-' __ -IiI "i'crnpetillUfC Refercflce Sensor J Dlfrl~rcnce (OF) C"I-') _ CF) in in, in, ------~~-------"--~.-------,~----.----~------------ Gt Type S Pitot Tube lnsp~"::lion Da.ta P" "" • LL t.l . .:.!.....--"".S~ __ in, ~ tJ.43 (~: « 1 0" G.: <: 10" Z ~:'l)_l::j in in C1: '" ~ __ ••. --,-l __ ~ 0: = ____ .9 __ Z= ,,0 ~) ~_tn Z -----~.III"""1- rr---·· _ .. -.----~ (--------.-.~-~ .. -" w ~ 00312:5 in. W'" 'OOLin w > ~j inchi:, in Z > :;/.\ inch L =: __ \ _____ il1 _""""" ___ .... """"" ...... ,_ ...... ___ ~j Am~CU2 ~ ___ .:...T\...::.:.'r-:.:.,:ij reratllr~ SCi1sor (~\1 tbr~~t()n ___ .. ___ .. ___ ._._ .. __ .. __ _ Probe: I ........ _ ,~ -AI" j~1D =Ii~1 /-. leE ~\, -\ T~~ "'I." __ <"~ -L _~ f St..l~k BOIL \\,,\ TERJf-_~..o .!i.. ~!:!-._: SILlCa>:E ~f--i _. ---', TETCO Sample Box 'rem perature Sensor Calibration Date: 12/29/11 Calibrator: ..:::.K;;:;.a.;",.~....:'a;;:;.i_rv..:::.1 .... cN--.:..a1..:::.11;;:;.a....:ra~ _________ _ Unit ID A B c D E F Thermocouple Location Oven Probe Out Impinger Out Oven Probe Out Impitlger Out Oven Probe Out Impinger Out Oven Probe Out Impinger Out Oven Probe Out Impinger Out Oven Probe Out Impinger Out Impinger Out G Impinger Out H Impinger Out I Impinger Out J Impinger Out K Reference: Omega CL3512A Temp.Oiff. or Resolt APPENDIXF The testing followed the same procedures as outlined in previous protoco]s and tests at this facility. ATTACHMENT H SURF ACE WATER GRAPHS AND FIELD DATA SHEETS Cottonwood Creek Dissolved Radionuclide Concentrations (uCi/ml) 1.00E-05 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ • 1.00E-06 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~§ - 1.00E-07 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~§ a; m • u • • i·OOE-OB ~~~~~~~~~~~~~~~~~[r~~~~:~~~:~~===~~!0 1 .00 E -09 t :::::::::::::.: ... : ... : ........................................ ~ ...... ~ ... ~ ... ~ ... ~ ........ ~ ..... ~ ... ~.::::::::::.::::::::::::::::::::::::::::::IE::::::::::........................................... . ............ 1: ... : ... : ... : ................................. :::::::::::::::::::::::::::.~:::::::::: :::::::::::::::::::::::::::::::::::::::::::::::i : ... ~:::::::::::::::.:::~::::::::::::::::::::::::=:::=::::::... :::::::::::::::::::==:::::=:=:::::::~~:::::::::::=:~=::::::::~:::-:I ::::::~~~~:~:==:~:::::=~:::~~~~ .. ~:::~~=.:::=~=-~=.::::::.~=.:::~~~-~~=~::~~=~=~=::=:::.~:::=~=:::::::=:::::::=.:::::::::::::::::::::::::::~::::::=::~~::=~:=.-::::::::::::.:::::~:::::::::::~:::::::::::::::::::~::: ........... :::.::::::::~::::::::::.::::::::::::.::.:::::::: .... ::::::::.:::::::.::::.:.::.::~........................................................... .............. ~:~::~::::::::~:::.::::~::::=::=~:::~:~~~=~=~~:~=~=::==.~ -.. =::!.~~:~~~;:=~= .. =~=~~~=~~:!==~=~ .. =~~==~=~~:~=:~~ .. ::::=:::::~~ ... :::~~:~:::::~::~;=:~~::~:;;::~~~:~ ... ::~:~:::~ •.. ·····:::·:::;::::;:·~:;::·~·:::~:~~~~·A··· .......... : .... .i •• ~~."~ ..... ~ ........ -~ .... ~~~~ .. ~=~~-===~=~~ 1.00E-1 0 ~==~::~~==::~=~c=~:~~::::~~::~~,~~.~~~.,::==.:::~~~~==~=.~=.~~~~:~~~~ ::~="':-::=.:=::~=.:::=:===:~~~~~ .. ~=::::::~:.~~:~: ~:~~~.=.~~i.~~.=j 1.00E-11 OJ'b~ ~~ ~ ~ ~,...Oj ~rf OjOjf1; ~~ :-...~ ,...'V R>'b ~,...Oj ~ro • U-Nat. -Th-230 .. Ra-226 ~~O::J ~~ ~fl, ,... ~ s:5 ~ <d-""Oj -- Cottonwood Creek Suspended Radionuclide Concentrations (uCi/ml) 1.00E-06 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ • 1.00E-07 §~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ ~=~=====~===~=====~=~=~=~=~==~~=======~-.~~~~=~===~=~=~=~=~.~~.======~=~=========:=~~====~~~~~~~=~~:~~~~~ .. ::~-:=~:=~=~====--.. _ ..... __ .......... _ .. _. __ ._ .. _--_ .. _ ..•. _ ..... _. __ ._ ....... _-... _ ... _._-_ .... _. __ . __ .- A • (.) • •• A ~ l 1·00E -0 9 ~~~=~~~~~;:~~~:::~~~-~~~~:·-;:.-:::=~~~~~3~E~~ ...........................•.... ......•..... . ....................................................................................................................... -.................................................................. _._ .... _ ...... _ .... _.-.. -•. _ .• -._--... .. 1.00E-10 §~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 1.00E-11 I-..:-.. -=-.. -::.~-=-.. -=-.. -::::.-=-.. -=-.. -::::.~ .. = .. -::.-::-..:-.. -=-.. -=--~~ .. -=-..:-.. -::::.-=--=-.. -::.~~:::--:::::~--=-.. -=-..:-.. -::::.-::::.-=-_-::::.-=-_-::::.-=-_-=-_-=-_-=-_-::::.-=--::::.-::::.-=-_-::::.-::::.-::.~-=-_-::::.-::.~-::::.-::::.-=-_-=-_-::::.-=-~:::-_-::::.-::.~:::-~::=~:::-_~~_-::.-::-~~_~~ ... ::::: . ..::-_~~~-::::=::-:=::~-.. ~::-::-::~-::-~~ .. -=-.. -::.~-::.-:::~_-:~_-=-_-:::~-::::::::-.. ~= ....... __ ... ___ .. _ ...... _ ... _ .... _ .. _._ .... _._ .. _ .. __ .. _ ..... _ .. ___ ....... _ ...........• 1.00E-12 +1----,----,----....,------,-----r-------r------,-------.-----.-------1 ~<o ~Oj ~~ ~ ~~Oj ~1' 2l<:;:) ~~Oj cJ.~ 2l0:> ~~Oj n}~ 2l<O ~~Oj ~~<o ~t'); 2lCO ~~Oj ~~r;:s ~~ cJ.cJ.rf • U-Nat. -Th-230 • Ra-226 ~~ n}rVrf ~c:o ~ ~ ~" ~OJ ~ q}o/ www.energylab.com Analytical Ext;8UBfICB Sines 7952 Helena, MT 877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 -1!jll~~a, wY:,8~6· .. GB6~7n5 • Rapid City, SI} 888-672-1225 • College Station, IX 888-690-2218 April 02, 2012 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C12030626 ANALYTICAL SUMMARY REPORT Project Name: 1 st Quarter Surface Water 2012 Energy Laboratories, Inc. Casper WY received the following 2 samples for Denison Mines USA Corp on 3/16/2012 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C12030626-001 Cottonwood Creek 03/12/12 12:45 03/16/12 Aqueous Solids, Total Dissolved Solids, Total Suspended C12030626-002 Temp Blank 03/15/12 0:00 03/16/12 Aqueous Temperature The analyses presented in this report were performed at Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601, unless otherwise noted. Radiochemistry analyses were performed at Energy Laboratories, Inc., 2325 Kerzell Lane, Casper, WY 82601, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. Data corrected for moisture content are typically noted as - dry on the report. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. If you have any questions regarding these test results, please call. Report Approved By: c3¥~ £; uJal~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2012.04.02 11 :31 :56 -06:00 Page 1 of 8 www.energylab.com Analytical ExcsIJsncIl SiRes 1952 _ _ .H,ef~na, ~B77-4l2-0711 • Billings, MT 800-735 .. 4489 • Gasper, WY 888-235-0515 . -GiUe{fe,WY:866-686-7175 . Raid City, SO 888-612-1225 • College Station, IX 888-690-2218 CLIENT: Denison Mines USA Corp Project: 1 st Quarter Surface Water 2012 Report Date: 04/02/12 Sample Delivery Group: C12030626 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 40C (±2OC) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay. Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors. When the results for all seven are NO (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SO eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001, Radiochemical WY200002; Utah: WY00002; Virginia: 00057; Washington: C836 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 2 of 8 EI\ERGY LABORATORIES www.energylab.com Analytical ExCBHtmCs Sine, 1952 ; ......• '. .•.. .;Hele~a, MTB17-412"0711 • Billings, MT 800-735-4489 . Casper, WV 888-235-0515 "' ... ·iijl~~~;'Wy'~6& .. G86~7j15 • Rapiq Cfty, S[} 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 1 st Quarter Surface Water 2012 C12030626-001 Client Sample 10: Cottonwood Creek Analyses PHYSICAL PROPERTIES Solids, Total Dissolved TDS @ 180 C Solids, Total Suspended TSS @ 105 C Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 224 15 o -Rl increased due to sample matrix. Units mg/l mg/l Report Date: 04/02/12 Collection Date: 03/12/12 12:45 DateReceived: 03/16/12 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By 10 A2540 C 03/19/12 08:59 / ab 0 6 A2540D 03/16/12 12:591 ab MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 3 of 8 EN:RGY LABORATORIES www.energylab.com Analytical ExcaIIsncll Sines 7952 ' ....... :HeI~,n,a,MT 8Jl-412-0J11 • Billings,MT 800-735-4489 • Casper, WY 888 .. 235-0515 ?jll~~~{WY<~8~6 .. $B6~711~ • R~pid City, SD 888-672-1225 • College Station, lX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 1 st Quarter Surface Water 2012 C 12030626-002 Client Sample ID: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Defi n itions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2.8 Qualifier Rl Report Date: 04/02/12 Collection Date: 03/15/12 DateReceived: 03/16/12 Matrix: Aqueous MCL! QCl Method Analysis Date / By E170.1 03/16/1209:35/ kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 8 EN:RGY LABORATORIES www.energylab.com Analytical ~t;BJIBfl&B SIncs 1952 !Hele~a, Mt'87l .. 472-0711 • Billings, MT 800-735~4489 . Casper, WY 888-235-0515 'Gill'ette, WY _8&6 .. 686~ 7115 • R~pip City, SD 88B~672~ 1225 • College Station, lX 888~69D~2218 ,-,,<,. ,,,. --. .~. QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1 st Quarter Surface Water 2012 Analyte Count Result Units Method: A2540 C Sample 10: MBLK1_120319 Solids, Total Dissolved TDS @ 180 C Sample 10: LCS1_120319 Solids, Total Dissolved TDS @ 180 C Sample 10: C12030630-001AMS Solids, Total Dissolved TDS @ 180 C Sample 10: C12030651-001AOUP Solids, Total Dissolved TDS @ 180 C Method Blank NO mg/L Laboratory Control Sample 1620 mg/L Sample Matrix Spike 2250 mg/L Sample Duplicate 2640 mg/L Report Date: 04/02/12 Work Order: C 12030626 RL %REC Low Limit High Limit RPO RPOLimit Qual Run: BAL .. 1_120319B 4 Run: BAL-1_120319B 10 97 90 110 Run: BAL-1 120319B 10 102 90 110 Run: BAL-1 120319B 10 Batch: 120319_1_SLDS-TDS-W 03/19/12 08:50 03/19/12 08:50 03/19/12 09:00 03/19/12 09:02 0.1 5 ---------------------------------------------------- Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. Page 5 of 8 EI\ERGY www.energylab.com .• ~ejen~.Mi.·~71 .. 472-071t .Billings.MT 800-735-4489 • Casper, WY 888-235-0515 AI/I1ytir;afExcsI'BflCBSiI1cs 1952 ~_ ~J~11~~~~WYJ.6~'~86-711~ '. Rapid City, SD 888-672·1225 • CollegeStation, IX 888-690·2218 LABORATORIES QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 1 st Quarter Surface Water 2012 Analyte Count Result Units Method: A2540 0 Sample 10: MBLK1_120316 Solids, Total Suspended TSS @ 105 C Method Blank ND mg/L Sample 10: LCS1_120316 Laboratory Control Sample Solids, Total Suspended TSS @ 105 C 177 mg/L Sample 10: C12030556-001 BOUP Sample Duplicate Solids, Total Suspended TSS @ 105 C 68.0 mg/L Qualifiers: RL -Analyte reporting limit. Report Date: 04/02/12 Work Order: C12030626 RL %REC Low Limit High Limit Run: BAL-1_120316A 2 Run: BAL-1_120316A 6.0 88 60 110 Run:BAL-1120316A 6.0 ND -Not detected at the reporting limit. RPO RPOLimit Qual Batch: 120316_1_SLDS-TSS-W 03/16/12 12:58 3.0 03/16/12 12:58 03/16/12 12:59 5 Page 6 of 8 Er\ERGY LABORATORIES ~1~· www.energylab.com ~ Analytfcal Excsllsncs Sine, 1952 _ / C .. .HejeM. M'T B17~412·071t • Billings, MT 800-735-4489 · Casper,WY 888 .. 235-0515 " ;,";~JiJ~~~, 'V~Y'lG6 .. ~86 .. 717~ • Rapid City; S[) 888-672-1225 • College Station, TX 888-690-2218 Workorder Receipt Checklist Denison Mines USA Corp 11111111111111 ~I~ 1111111111111111111111 C12030626 Login completed by: Kristy Gisse Reviewed by: BL2000\kschroeder Reviewed Date: 3/16/2012 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res CI, Sulfite, Ferrous Iron, etc.) ContaineriTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments: None Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 2.8"C On Ice Yes D Yes 0 Date Received: 3/16/2012 Received by: dw Carrier FedEx name: No D No D No D No D No D No D No D No D No D No D No D No D Not Present D Not Present D Not Present 0 No VOA vials submitted 0 Not Applicable D Page 7 of 8 "'U 0,) lU.i'fftY Chain of Custody and Analytical Request Record Page __ of __ •• m.mlJIJI»),.Z. PLEASE PRINT (Provide as much information as possible.) Company Name:.o • M~A~ Project Name, PWS. Permit, Etc. ~t"-Sample Origin EPA/State Compliance: ~,.s(")tI\. 15+ Qv~+e.c-S •. 1I'·f~ WD...\-e.r Yes $ No 0 State: VT Report Mail Address: " Lf ~ 5. \+t...)t ''ll Contact Name: Phone/Fax: Email: Sampler: (Please Print) ~\~\~1 vr g~511 rr~u-tl-()'l~ol~y l..I3S -67 f -::z.:2:;1 \ ~,~ I>~\~"'" Invoice Address: InVOice Contact & Phone: Purchase Order: Quote/Bottle Order: S~Me-(1tw5 f>...,bdVe->~ A..S t.1o-bollt- Special Report/Formats: 3: ~ W@D® OO~®QDrn@lJrn@) .... Contact ELI prior to l~~ 0 (j) RUSH sample submittal ~O(/).s=. for charges and Cooler IO{s): .' ~1ll~OI 03 ~ R ~l{\~-0 scheduling -See ._> 0 >-ro W t-I nstruction Page Dow D EDD/EOT(Electronic Data) .19 (/) Cf.) <t1 s: '-" c (), (/) :r: '0 DpOTWIWWTP 03:= ~ 0') 0 c Comments: iLtW °C Format: ~«~1.2 ~ :::J U ~ a o State: o LEVEL IV o ,-all c: ... ... Q).ffi c:-c. m -~~I~'? ~ c Ci> o Other: D NELAC ~ On Ice: :::J :J Q,).: 1i) 3: t-5 z15..<1:1 arD W "0 Custody Seal '-!ij >1 W (tI On Bottle Y N CI) '0 Y N Cf.) c On Cooler V1 ~ (tI 0 Ci5 H Intact Y N SAMPLE IDENTIFICATION Collection Collection MATRIX t-J-Signature Y N (Name, Location, Interval, etcl Date Time Match 1 \~45 1-t,J )t. X C. o++cA"""occl C r~e.,," ~-I~-3.0l~ I~ 2 .~ 3 :g Innn 4 ~ 5 I~ ~ 6 ~ 7 ,~ C. \ ')o.3D' ~~ B ~ I 9 l!l 10 i~ Custody Relinquished by (print): DatelTime: SignaLre: _ p~ Received by (print): DatelTime: Signature: 6.,..,...-."" P .. '~t'" ~-15"1~ J \100 Record J.,iI"'!"'" Relinquished by (print): Date/Time: Signature: Received by (print): D atelTi me: Signature: MUST be Signed Sal11Ple D iSP9sal: Return to Client Lab Disposal: \L1 r<' by L8uoraW7Jl1 u~me: /1,. / ~ t 1\ r '..I . .,fo~/1 --2-SignOtre: ~ s- t o~r certified laboratories in order to complete the analysis requested. In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted tc pOSSIOllity. An sub-contract data will be~rly notated on your analytical rep Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. Cottonwood Creek was dry during the second quarter of 2012. No samples were taken. White Mesa MilI-Standard Operating Procedures Book #11: Environmental Protection Manua), Section 2.1 ) Date: 2/07 Revision: DUSA-l Page50f5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one:(£Ott~nwood s!~i:)westwater Canyo~ Other (describe) ___ _ pH BUFFER 7.o_-",,"-7.;,.,.;;p 0=---__ BY: GP (Sampler's initials) pH BUFFER 4.0 _Y.o..;... ,,:;,0 __ _ SPECIFIC CONDUCTIVITY _ ..... i ..... Q ....... 9 _____ ....... u=MH==.;O=s STEAM DEPTH: L.I i \ --~-------------- pHofWATER ___ -Z~~~5~·~I ________ _ COND umhos 6° 7 5 pH Units 7~g6 Temp °c _-:q_._~.-;..I __ COND J1m!!o~_.6 7 4 pH units 7 ., g~ TempoC Comments: CONDJ.l:mhos 67L{ pH units ·7" 2~ .. Temp °C .. Cf . -:l ~.. COND J.lmhOS .. t 7·3 pH units __ 7~._f/...;;.5 __ Temp °c __ q.:....#;....7~q..L.__ ~A.t't--'v~ p""" .s;t~ A.J: ,:lSSr 6c)..tf'.~:~ .~ r{\;6v\.~fN:;·>Mt-eet S,;\.tV\t tl~ .eu,44t,~Arp..tAe..±er.s W4f'C ' +" .. \6.~,-?~~ples Wue tkt.,A c.,.ot\e..c.A cl t.t+ l;2f!:15 .. id ~l)..tl-..e.: .. ~+ hu""'"~ e>9 . .J:~,v\t2 t ;~.~e:...s $~(\,~i . w 'f.k f!4-~e'~-h4'c.. ()f 'Sot..;. kJ&~ .. Aer {~ -\-L....c.. v-r~l. wv....S jAAo.s+ly c:...l"A.C' A.~ u.J.s+vrbut - ! ~ f '. !;t. White Mesa Mill -Standard Operating Procedures Book #11: Environmental Protection Manual, Section 2. I Date: 2107 Revision: DUSA-l PageS of5 Attachment A FIELD WATER ANALYSIS SURFACE WATER WHITE MESA MILL LOCATION (Circle one)Qtionwood ci;k:? Westwater Canyon Other (describe ) ___ _ DATE: t/()6/';'" pH BUFFER 7.0 _ ........ 7:....r.c..}..,Q~ __ BY: GAn-'I" p~.Jvvte,.-{t-.ej (Sampler's initials) pH BUFFER 4.0 __ L1..;..:..<-..;:;;;O'---__ _ SPECIFIC CONDUCTIVITY _~q:.......;1~q.l.....-____ -.cH=MH=O=S STEAM DEPTH: o pH ofWATER __ ~ _______ _ TEMP ____________ _ , , COND ~umh=o=s~ ___ _ COND Il=mh=----os _______ _ pH Units ______ _ pH units ______ _ Temp °c ______ _ Temp °c ______ _ COND~=rr.ili==os~ ______ __ COND ~=mh=os:::..._ ____ _ pH units ________ _ pH units __________ _ Temp °c __________ _ Temp °c _______ _ Comments: ()I;.+lp...r b Ute 2.~ c-..f.t-e.Mpt 1/1 f/J ~, An,·vc.J.... 0 r.... $/'[ e ~I-130f), Lt'c..e t. (...)?kS ,1 (" 1 s ~e... 4 t tAG~, ? rJ... "'--t-~ kAft 612.6/ t:2.. f Ar r ~ v'~A () A-.s J' fc. 0....+ 1300, t:.-rl:.t.k.-.sf;/{ tAr-i-'T;..,AV\.c:.r !+oll:J.A.Y ~ Ge-r;-I ........ fi\..ll'VI-e.I (J"""'" s~+C-.ro-r-a-tl tvl·t~p~.st ATTACHMENT I SOIL SAMPLE GRAPHS, DATA TABLE, LABORATORY RESULTS AND QAIQC Soil samples are collected during the third quarter. This attachment has been deliberately left blank.